ap-3-12.dvi Acta Polytechnica Vol. 52 No. 3/2012 Resistance Spot Welding of dissimilar Steels Ladislav Kolař́ık1, Miroslav Sahul2, Marie Kolař́ıková1, Martin Sahul3, Milan Turňa2, Michal Felix4 1 Czech Technical University in Prague, Department of Manufacturing Technology, Technická 4, 166 07 Praha, Czech Republic 2 Slovak University of Technology, Department of Welding, Pauĺınska 16, 917 24 Trnava, Slovak Republic 3 Slovak University of Technology, Department of Materials Engineering, Pauĺınska 16, 917 24 Trnava, Slovak Republic 4 Fronius Česká republika, s. r. o, Dolnoměcholupská 1535/14, 102 00 Praha, Czech Republic Correspondence to: Ladislav.Kolarik@fs.cvut.cz Abstract This paper presents an analysis of the properties of resistance spot welds between low carbon steel and austenitic CrNi stainless steel. The thickness of the welded dissimilar materials was 2 mm. A DeltaSpot welding gun with a process tape was used for welding the dissimilar steels. Resistance spot welds were produced with various welding parameters (welding currents ranging from 7 to 8 kA). Light microscopy, microhardness measurements across the welded joints, and EDX analysis were used to evaluate the quality of the resistance spot welds. The results confirm the applicability of DeltaSpot welding for this combination of materials. Keywords: resistance spot welding, welded joint, low carbon steel, austenitic stainless steel. 1 Introduction Several problems arise when welding dissimilar steels, related mainly to the different physical, chemical and mechanical properties of the welded materials. Austenitic stainless steel and low carbon steel possess a good combination of mechanical properties, forma- bility, weldability and resistance to corrosion. This combination of steels is extensively used in the power generation industry [1,2]. Research on welding is car- ried out at various research institutions [3, 4]. The aim of our paper is to analyze and compare the prop- erties of resistance spot welds of low carbon steel and austenitic stainless steel. Optical microscopy, micro- hardness measurements and EDX analysis were used to analyse the properties of the spot welded joints. 2 Experimental The welded materials used for resistance spot weld- ing were DC 01 low carbon steel (LCS) and AISI 304 austenitic stainless steel (ASS). The welded steels were 2 mm thick. Both metals were delivered in cold rolled state. The chemical composition of the steels is given in Tables 1 and 2. It was necessary to take various properties of the welded metals into consider- ation, e.g. thermal conductivity and electrical resis- tivity. The thermal conductivity of ASS and LCS is about 16.2 W·m−1·K−1 and 52 W·m−1·K−1, respec- tively. Differences in the properties of the metals re- sulted in an asymmetrical weld nugget. The electrical resistivity of ASS is approximately 72 μΩ · cm, while the electrical resistivity of LCS is 14.2 μΩ · cm [6]. Table 1: Chemical composition of DC 01 low carbon steel Main alloying elements [wt. %] C Mn P S ≤ 0.12 ≤ 0.60 ≤ 0.045 ≤ 0.045 Table 2: Chemical composition of AISI 304 austenitic stainless steel Main alloying elements [wt. %] C ≤ 0.07 Cr 17.0 to 19.5 Ni 8.0 to 10.5 Mn ≤ 2.00 Si ≤ 0.045 P ≤ 0.045 S ≤ 0.015 N ≤ 0.11 43 Acta Polytechnica Vol. 52 No. 3/2012 Resistance spot welds were produced at the Fro- nius Technology Centre in Prague, in cooperation with the Faculty of Mechanical Engineering, Czech Technical University in Prague. The DeltaSpot sys- tem by Fronius was used for producing the resistance spot welds. DeltaSpot is a welding gun (Figure 1) with a running process tape (type PT 3200-CrNi and PT 1200-steel) that protects the electrodes (R+100 and R+500, �16 mm) from wear and deposits of sheet coatings. The welding current used in the experiment ranged from 7 to 8 kA. The other parameters were kept constant. The welding parameters are given in Table 3. Figure 1: DeltaSpot X-Gun (left) and a detail of the process tapes (right) [5] Table 3: Parameters for welding dissimilar steels Sample code Welding current Welding current cycle duration Force Force cycle duration [ms] [kA] [ms] [kN] [ms] 1 8.0 370 4.0/3.4 310/480 2 7.5 370 4.0/3.4 310/480 3 7.0 370 4.0/3.4 310/480 Figure 2: Example of a welding cycle — Dependence of welding current and force on time 44 Acta Polytechnica Vol. 52 No. 3/2012 Figure 3: Verification of the weld nugget size (left) and the macrostructure of a selected dissimilar resistance spot weld (IW = 7.5 kA) Figure 4: HAZ – DC 01 steel interface The quality of the weld joins was proved by peel testing (EN ISO 10 447), see Figure 3 – left. The size of the weld nugget was measured. Sample 2 was chosen for further analysis. Light microscopy (for analysing the macro- and microstructures of the welds), microhardness mea- surements across the welded joints, and EDX analysis were used to analyse the properties of the resistance spot welds that were produced. The macrostructure of the welded joint produced by using a welding cur- rent of 7.5 kA is documented in Figure 3. As the macrostructure suggests, the welded joint is asym- metrical. The fusion zone size on the stainless steel side is larger than the fusion zone on the low car- bon steel side. Similar results were also observed in welds produced with welding currents of 7 and 8 kA. The heat-affected zone (HAZ) of the DC 01 steel is broader due to the higher thermal conductivity of the low carbon steel sheet. On the basis of macrostruc- ture analysis, it can be stated that the higher the welding current that is used, the larger the fusion zone. The microstructure of low carbon steel is fully fer- ritic. Grain refining was observed in the low temper- ature HAZ of carbon steel (Figure 4). Some amounts of pearlite were also present. Grain coarsening oc- curred in the high temperature HAZ of carbon steel. Figure 5: SEM image of a dissimilar steels weld nugget Figure 6: SEM image of base materials and a welded joint 45 Acta Polytechnica Vol. 52 No. 3/2012 The structure of the weld nugget obtained by scanning electron microscopy is presented in Figure 6. A JEOL 7600 F scanning electron microscope with a field emission gun fitted with an X-Max 50 mm2 EDX detector was used to obtain images and for EDX anal- ysis. The observation parameters were: accelerating voltage 20 keV, probe current 2 nA and working dis- tance 15 mm. A more detailed view of the welded joint produced with a welding current of 8.0 kA is shown in Figure 6. Figure 7: Course of microhardness across a welded joint (IW = 7.5 kA) Vickers microhardness measurements across the weld nugget were performed on each sample. The in- dividual indents were made horizontally, in two rows (AISI 304 steel and DC 01 steel, respectively). The first one was done in austenitic stainless steel across the weld nugget and the other in low carbon steel through HAZ and the weld nugget. The distance be- tween the indents in the weld metal was 500 μm. The distance between the indents in the base metals and HAZ was 200 μm. The loading used in the experi- mental measurements was 100 g, acting over a period of 10 s. The hardness measurement results are given in Figure 7. EDX analysis was used for a more detailed study of the welded joint — base metal interface. The area examined by EDX analysis, and also the line profiles of Cr, Ni, Mn and Fe elements are given in Figure 8. 3 Conclusion The properties of resistance spot welds of dissimi- lar steels have been studied. The influence of the welding parameters on the weld metal size has been evaluated. The size of the weld metal increases with welding current increase. The HAZ of the low car- bon steel sheet was broader than the HAZ of the austenitic stainless steel. This is related to the higher thermal conductivity of DC 01 steel. The structure of low carbon steel is fully ferritic. AISI 304 steel con- sists of austenitic grains with the presence of twins. Grain refining of ferrite grains was observed in the low temperature HAZ at carbon steel. The hardness increased in the fusion zone. In low carbon steel, the increase was from a value of 131 HV0.1, mea- sured in the base metal, to hardness of 367.9 HV0.1 (measured in the weld metal). A similar perceptible increase was attained in stainless steel sheet. The hardness measured in AISI 304 steel increased from a value of 186.9 HV0.1 to a value of 359.9 HV0.1. A more detailed study of the welded joint interface was performed by EDX analysis. An increase in iron con- tent in the direction from weld metals towards DC 01 steel was observed. However, a decrease in Cr, Mn and Ni from the weld metal towards the DC 01 steel was also recorded. Figure 8: a) Area studied using EDX analysis, b) line profiles of Cr, Ni, Mn and Fe across the weld metal — DC 01 steel interface (IW = 7.5 kA) 46 Acta Polytechnica Vol. 52 No. 3/2012 Acknowledgement The paper was prepared with support from the Grant Agency of the Ministry of Education, Sci- ence, Research and Sport of the Slovak Republic and the Slovak Academy of Sciences within project No. 1/2594/12. The research was financed by the Czech Ministry of Education, Youth and Sport within the framework of project SGS CVUT 2010 — OHK2-038/10. References [1] Arivazhagan, N., Singh, S., Prakash, S., Red- dy, G. M.: Investigation on AISI 304 Austenitic Stainless Steel to AISI 4140 Low Alloy Steel Dissimilar Joints by Gas Tungsten Arc, Elec- tron Beam and Friction Welding. In Materials and Design 2011. Elsevier, p. 3 036–3 050. ISSN 0261-3069. [2] Krishnaprasad, K., Prakash, R. 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