id	sid	tid	token	lemma	pos
admet-249	1	1	manuscript	manuscript	PROPN
admet-249	1	2	doi	doi	PROPN
admet-249	1	3	:	:	PUNCT
admet-249	1	4	10.5599	10.5599	NUM
admet-249	1	5	/	/	SYM
admet-249	1	6	admet.3.4.249	admet.3.4.249	NOUN
admet-249	1	7	352	352	NUM
admet-249	1	8	admet	admet	X
admet-249	1	9	&	&	CCONJ
admet-249	1	10	dmpk	dmpk	PROPN
admet-249	1	11	3(4	3(4	NUM
admet-249	1	12	)	)	PUNCT
admet-249	1	13	(	(	PUNCT
admet-249	1	14	2015	2015	NUM
admet-249	1	15	)	)	PUNCT
admet-249	1	16	352	352	NUM
admet-249	1	17	-	-	SYM
admet-249	1	18	358	358	NUM
admet-249	1	19	;	;	PUNCT
admet-249	1	20	doi	doi	NOUN
admet-249	1	21	:	:	PUNCT
admet-249	1	22	10.5599	10.5599	NUM
admet-249	1	23	/	/	SYM
admet-249	1	24	admet.3.4.249	admet.3.4.249	NOUN
admet-249	1	25	open	open	ADJ
admet-249	1	26	access	access	NOUN
admet-249	1	27	:	:	PUNCT
admet-249	1	28	issn	issn	PROPN
admet-249	1	29	:	:	PUNCT
admet-249	1	30	1848	1848	NUM
admet-249	1	31	-	-	SYM
admet-249	1	32	7718	7718	NUM
admet-249	1	33	http://www.pub.iapchem.org/ojs/index.php/admet/index	http://www.pub.iapchem.org/ojs/index.php/admet/index	NOUN
admet-249	1	34	original	original	ADJ
admet-249	1	35	scientific	scientific	ADJ
admet-249	1	36	paper	paper	NOUN
admet-249	1	37	rapid	rapid	ADJ
admet-249	1	38	identification	identification	NOUN
admet-249	1	39	of	of	ADP
admet-249	1	40	bioactive	bioactive	PROPN
admet-249	1	41	carbohydrazide	carbohydrazide	PROPN
admet-249	1	42	reaction	reaction	NOUN
admet-249	1	43	products	product	NOUN
admet-249	1	44	by	by	ADP
admet-249	1	45	an	an	DET
admet-249	1	46	lc	lc	PROPN
admet-249	1	47	-	-	PUNCT
admet-249	1	48	dad	dad	NOUN
admet-249	1	49	-	-	PUNCT
admet-249	1	50	spe	spe	PROPN
admet-249	1	51	-	-	PUNCT
admet-249	1	52	nmr	nmr	NOUN
admet-249	1	53	approach	approach	NOUN
admet-249	1	54	iva	iva	PROPN
admet-249	1	55	habinovec	habinovec	PROPN
admet-249	1	56	,	,	PUNCT
admet-249	1	57	tomislav	tomislav	NOUN
admet-249	1	58	jednačak	jednačak	NOUN
admet-249	1	59	and	and	CCONJ
admet-249	1	60	predrag	predrag	PROPN
admet-249	1	61	novak	novak	PROPN
admet-249	1	62	*	*	PROPN
admet-249	1	63	university	university	PROPN
admet-249	1	64	of	of	ADP
admet-249	1	65	zagreb	zagreb	PROPN
admet-249	1	66	,	,	PUNCT
admet-249	1	67	faculty	faculty	NOUN
admet-249	1	68	of	of	ADP
admet-249	1	69	science	science	NOUN
admet-249	1	70	,	,	PUNCT
admet-249	1	71	department	department	NOUN
admet-249	1	72	of	of	ADP
admet-249	1	73	chemistry	chemistry	NOUN
admet-249	1	74	,	,	PUNCT
admet-249	1	75	horvatovac	horvatovac	PROPN
admet-249	1	76	102a	102a	PROPN
admet-249	1	77	,	,	PUNCT
admet-249	1	78	10000	10000	NUM
admet-249	1	79	zagreb	zagreb	PROPN
admet-249	1	80	,	,	PUNCT
admet-249	1	81	croatia	croatia	PROPN
admet-249	1	82	ihabinovec@chem.pmf.hr	ihabinovec@chem.pmf.hr	VERB
admet-249	1	83	;	;	PUNCT
admet-249	1	84	tjednacak@chem.pmf.hr	tjednacak@chem.pmf.hr	X
admet-249	1	85	*	*	PUNCT
admet-249	1	86	corresponding	correspond	VERB
admet-249	1	87	author	author	NOUN
admet-249	1	88	:	:	PUNCT
admet-249	1	89	e	e	NOUN
admet-249	1	90	-	-	NOUN
admet-249	1	91	mail	mail	NOUN
admet-249	1	92	:	:	PUNCT
admet-249	1	93	pnovak@chem.pmf.hr	pnovak@chem.pmf.hr	NOUN
admet-249	1	94	;	;	PUNCT
admet-249	1	95	tel	tel	PROPN
admet-249	1	96	.	.	PUNCT
admet-249	1	97	:	:	PUNCT
admet-249	2	1	+385	+385	PROPN
admet-249	2	2	-	-	SYM
admet-249	2	3	1	1	NUM
admet-249	2	4	-	-	PUNCT
admet-249	2	5	460	460	NUM
admet-249	2	6	-	-	SYM
admet-249	2	7	6184	6184	NUM
admet-249	2	8	;	;	PUNCT
admet-249	2	9	fax	fax	NOUN
admet-249	2	10	:	:	PUNCT
admet-249	2	11	+385	+385	PROPN
admet-249	2	12	-	-	SYM
admet-249	2	13	1	1	NUM
admet-249	2	14	-	-	PUNCT
admet-249	2	15	460	460	NUM
admet-249	2	16	-	-	SYM
admet-249	2	17	6181	6181	NUM
admet-249	2	18	received	receive	VERB
admet-249	2	19	:	:	PUNCT
admet-249	2	20	november	november	PROPN
admet-249	2	21	09	09	NUM
admet-249	2	22	,	,	PUNCT
admet-249	2	23	2015	2015	NUM
admet-249	2	24	;	;	PUNCT
admet-249	2	25	revised	revise	VERB
admet-249	2	26	:	:	PUNCT
admet-249	2	27	december	december	PROPN
admet-249	2	28	24	24	NUM
admet-249	2	29	,	,	PUNCT
admet-249	2	30	2015	2015	NUM
admet-249	2	31	;	;	PUNCT
admet-249	2	32	published	publish	VERB
admet-249	2	33	:	:	PUNCT
admet-249	2	34	december	december	PROPN
admet-249	2	35	30	30	NUM
admet-249	2	36	,	,	PUNCT
admet-249	2	37	2015	2015	NUM
admet-249	2	38	abstract	abstract	ADJ
admet-249	2	39	on	on	ADP
admet-249	2	40	-	-	PUNCT
admet-249	2	41	line	line	NOUN
admet-249	2	42	coupling	coupling	NOUN
admet-249	2	43	of	of	ADP
admet-249	2	44	high	high	ADJ
admet-249	2	45	performance	performance	NOUN
admet-249	2	46	liquid	liquid	NOUN
admet-249	2	47	chromatography	chromatography	NOUN
admet-249	2	48	with	with	ADP
admet-249	2	49	diode	diode	NOUN
admet-249	2	50	array	array	NOUN
admet-249	2	51	detection	detection	NOUN
admet-249	2	52	to	to	ADP
admet-249	2	53	solid	solid	ADJ
admet-249	2	54	phase	phase	NOUN
admet-249	2	55	extraction	extraction	NOUN
admet-249	2	56	combined	combine	VERB
admet-249	2	57	with	with	ADP
admet-249	2	58	nuclear	nuclear	ADJ
admet-249	2	59	magnetic	magnetic	ADJ
admet-249	2	60	resonance	resonance	NOUN
admet-249	2	61	(	(	PUNCT
admet-249	2	62	lc	lc	PROPN
admet-249	2	63	-	-	PUNCT
admet-249	2	64	dad	dad	NOUN
admet-249	2	65	-	-	PUNCT
admet-249	2	66	spe	spe	NOUN
admet-249	2	67	-	-	PUNCT
admet-249	2	68	nmr	nmr	NOUN
admet-249	2	69	)	)	PUNCT
admet-249	2	70	was	be	AUX
admet-249	2	71	used	use	VERB
admet-249	2	72	to	to	PART
admet-249	2	73	monitor	monitor	VERB
admet-249	2	74	carbohydrazide	carbohydrazide	ADJ
admet-249	2	75	condensation	condensation	NOUN
admet-249	2	76	reaction	reaction	NOUN
admet-249	2	77	progress	progress	NOUN
admet-249	2	78	.	.	PUNCT
admet-249	3	1	first	first	ADV
admet-249	3	2	,	,	PUNCT
admet-249	3	3	a	a	DET
admet-249	3	4	chromatographic	chromatographic	ADJ
admet-249	3	5	method	method	NOUN
admet-249	3	6	was	be	AUX
admet-249	3	7	developed	develop	VERB
admet-249	3	8	and	and	CCONJ
admet-249	3	9	optimised	optimise	VERB
admet-249	3	10	and	and	CCONJ
admet-249	3	11	individual	individual	ADJ
admet-249	3	12	peak	peak	NOUN
admet-249	3	13	separation	separation	NOUN
admet-249	3	14	was	be	AUX
admet-249	3	15	readily	readily	ADV
admet-249	3	16	achieved	achieve	VERB
admet-249	3	17	by	by	ADP
admet-249	3	18	using	use	VERB
admet-249	3	19	an	an	DET
admet-249	3	20	isocratic	isocratic	ADJ
admet-249	3	21	acetonitrile	acetonitrile	ADJ
admet-249	3	22	-	-	PUNCT
admet-249	3	23	phosphate	phosphate	NOUN
admet-249	3	24	buffer	buffer	NOUN
admet-249	3	25	mobile	mobile	ADJ
admet-249	3	26	phase	phase	NOUN
admet-249	3	27	.	.	PUNCT
admet-249	4	1	subsequently	subsequently	ADV
admet-249	4	2	,	,	PUNCT
admet-249	4	3	separated	separate	VERB
admet-249	4	4	compounds	compound	NOUN
admet-249	4	5	were	be	AUX
admet-249	4	6	trapped	trap	VERB
admet-249	4	7	on	on	ADP
admet-249	4	8	spe	spe	ADJ
admet-249	4	9	cartridges	cartridge	NOUN
admet-249	4	10	and	and	CCONJ
admet-249	4	11	dried	dry	VERB
admet-249	4	12	with	with	ADP
admet-249	4	13	nitrogen	nitrogen	NOUN
admet-249	4	14	gas	gas	NOUN
admet-249	4	15	.	.	PUNCT
admet-249	5	1	peak	peak	NOUN
admet-249	5	2	elution	elution	NOUN
admet-249	5	3	was	be	AUX
admet-249	5	4	then	then	ADV
admet-249	5	5	performed	perform	VERB
admet-249	5	6	with	with	ADP
admet-249	5	7	deuterated	deuterate	VERB
admet-249	5	8	acetonitrile	acetonitrile	NOUN
admet-249	5	9	and	and	CCONJ
admet-249	5	10	sent	send	VERB
admet-249	5	11	for	for	ADP
admet-249	5	12	nmr	nmr	NOUN
admet-249	5	13	analysis	analysis	NOUN
admet-249	5	14	.	.	PUNCT
admet-249	6	1	single	single	ADJ
admet-249	6	2	and	and	CCONJ
admet-249	6	3	multiple	multiple	ADJ
admet-249	6	4	trapping	trap	VERB
admet-249	6	5	options	option	NOUN
admet-249	6	6	were	be	AUX
admet-249	6	7	applied	apply	VERB
admet-249	6	8	.	.	PUNCT
admet-249	7	1	oneand	oneand	CCONJ
admet-249	7	2	two	two	NUM
admet-249	7	3	-	-	PUNCT
admet-249	7	4	dimensional	dimensional	ADJ
admet-249	7	5	nmr	nmr	NOUN
admet-249	7	6	spectra	spectra	NOUN
admet-249	7	7	were	be	AUX
admet-249	7	8	recorded	record	VERB
admet-249	7	9	using	use	VERB
admet-249	7	10	a	a	DET
admet-249	7	11	prodigy	prodigy	NOUN
admet-249	7	12	cryoprobe	cryoprobe	NOUN
admet-249	7	13	.	.	PUNCT
admet-249	8	1	it	it	PRON
admet-249	8	2	was	be	AUX
admet-249	8	3	demonstrated	demonstrate	VERB
admet-249	8	4	that	that	SCONJ
admet-249	8	5	lc	lc	PROPN
admet-249	8	6	-	-	PUNCT
admet-249	8	7	dad	dad	NOUN
admet-249	8	8	-	-	PUNCT
admet-249	8	9	spe	spe	NOUN
admet-249	8	10	-	-	PUNCT
admet-249	8	11	nmr	nmr	NOUN
admet-249	8	12	setup	setup	NOUN
admet-249	8	13	was	be	AUX
admet-249	8	14	proved	prove	VERB
admet-249	8	15	very	very	ADV
admet-249	8	16	useful	useful	ADJ
admet-249	8	17	for	for	ADP
admet-249	8	18	rapid	rapid	ADJ
admet-249	8	19	and	and	CCONJ
admet-249	8	20	unambiguous	unambiguous	ADJ
admet-249	8	21	identification	identification	NOUN
admet-249	8	22	of	of	ADP
admet-249	8	23	the	the	DET
admet-249	8	24	reaction	reaction	NOUN
admet-249	8	25	products	product	NOUN
admet-249	8	26	and	and	CCONJ
admet-249	8	27	for	for	ADP
admet-249	8	28	determination	determination	NOUN
admet-249	8	29	of	of	ADP
admet-249	8	30	their	their	PRON
admet-249	8	31	structure	structure	NOUN
admet-249	8	32	.	.	PUNCT
admet-249	9	1	by	by	ADP
admet-249	9	2	using	use	VERB
admet-249	9	3	prodigy	prodigy	NOUN
admet-249	9	4	cryoprobe	cryoprobe	NOUN
admet-249	9	5	in	in	ADP
admet-249	9	6	nmr	nmr	NOUN
admet-249	9	7	measurements	measurement	NOUN
admet-249	9	8	we	we	PRON
admet-249	9	9	were	be	AUX
admet-249	9	10	able	able	ADJ
admet-249	9	11	to	to	PART
admet-249	9	12	detect	detect	VERB
admet-249	9	13	and	and	CCONJ
admet-249	9	14	identify	identify	VERB
admet-249	9	15	compounds	compound	NOUN
admet-249	9	16	present	present	ADJ
admet-249	9	17	at	at	ADP
admet-249	9	18	microgram	microgram	ADJ
admet-249	9	19	level	level	NOUN
admet-249	9	20	thus	thus	ADV
admet-249	9	21	proving	prove	VERB
admet-249	9	22	a	a	DET
admet-249	9	23	high	high	ADJ
admet-249	9	24	sensitivity	sensitivity	NOUN
admet-249	9	25	of	of	ADP
admet-249	9	26	this	this	DET
admet-249	9	27	methodology	methodology	NOUN
admet-249	9	28	for	for	ADP
admet-249	9	29	monitoring	monitor	VERB
admet-249	9	30	reactions	reaction	NOUN
admet-249	9	31	of	of	ADP
admet-249	9	32	bioactive	bioactive	ADJ
admet-249	9	33	molecules	molecule	NOUN
admet-249	9	34	and	and	CCONJ
admet-249	9	35	drugs	drug	NOUN
admet-249	9	36	.	.	PUNCT
admet-249	10	1	keywords	keyword	NOUN
admet-249	10	2	carbohydrazide	carbohydrazide	VERB
admet-249	10	3	derivatives	derivative	NOUN
admet-249	10	4	;	;	PUNCT
admet-249	10	5	reaction	reaction	NOUN
admet-249	10	6	monitoring	monitoring	NOUN
admet-249	10	7	;	;	PUNCT
admet-249	10	8	lc	lc	PROPN
admet-249	10	9	-	-	PUNCT
admet-249	10	10	dad	dad	NOUN
admet-249	10	11	-	-	PUNCT
admet-249	10	12	spe	spe	NOUN
admet-249	10	13	-	-	PUNCT
admet-249	10	14	nmr	nmr	NOUN
admet-249	10	15	;	;	PUNCT
admet-249	10	16	product	product	NOUN
admet-249	10	17	identification	identification	NOUN
admet-249	10	18	;	;	PUNCT
admet-249	10	19	structure	structure	NOUN
admet-249	10	20	elucidation	elucidation	NOUN
admet-249	10	21	introduction	introduction	NOUN
admet-249	10	22	aromatic	aromatic	ADJ
admet-249	10	23	imines	imine	NOUN
admet-249	10	24	derived	derive	VERB
admet-249	10	25	from	from	ADP
admet-249	10	26	carbohydrazide	carbohydrazide	NOUN
admet-249	10	27	are	be	AUX
admet-249	10	28	promising	promise	VERB
admet-249	10	29	therapeutic	therapeutic	ADJ
admet-249	10	30	agents	agent	NOUN
admet-249	10	31	with	with	ADP
admet-249	10	32	a	a	DET
admet-249	10	33	broad	broad	ADJ
admet-249	10	34	spectrum	spectrum	NOUN
admet-249	10	35	of	of	ADP
admet-249	10	36	biological	biological	ADJ
admet-249	10	37	properties	property	NOUN
admet-249	10	38	,	,	PUNCT
admet-249	10	39	such	such	ADJ
admet-249	10	40	as	as	ADP
admet-249	10	41	antiviral	antiviral	ADJ
admet-249	10	42	,	,	PUNCT
admet-249	10	43	antitubercular	antitubercular	ADJ
admet-249	10	44	,	,	PUNCT
admet-249	10	45	antifungal	antifungal	ADJ
admet-249	10	46	,	,	PUNCT
admet-249	10	47	cytotoxic	cytotoxic	ADJ
admet-249	10	48	and	and	CCONJ
admet-249	10	49	antimalarial	antimalarial	ADJ
admet-249	10	50	activity	activity	NOUN
admet-249	10	51	[	[	X
admet-249	10	52	14	14	NUM
admet-249	10	53	]	]	PUNCT
admet-249	10	54	.	.	PUNCT
admet-249	11	1	furthermore	furthermore	ADV
admet-249	11	2	,	,	PUNCT
admet-249	11	3	they	they	PRON
admet-249	11	4	were	be	AUX
admet-249	11	5	reported	report	VERB
admet-249	11	6	to	to	PART
admet-249	11	7	be	be	AUX
admet-249	11	8	used	use	VERB
admet-249	11	9	as	as	ADP
admet-249	11	10	precursors	precursor	NOUN
admet-249	11	11	in	in	ADP
admet-249	11	12	the	the	DET
admet-249	11	13	synthesis	synthesis	NOUN
admet-249	11	14	of	of	ADP
admet-249	11	15	various	various	ADJ
admet-249	11	16	nitrogen	nitrogen	NOUN
admet-249	11	17	and	and	CCONJ
admet-249	11	18	sulphur	sulphur	NOUN
admet-249	11	19	containing	contain	VERB
admet-249	11	20	heterocycles	heterocycle	NOUN
admet-249	12	1	[	[	X
admet-249	12	2	5,6	5,6	NUM
admet-249	12	3	]	]	PUNCT
admet-249	12	4	.	.	PUNCT
admet-249	13	1	owing	owe	VERB
admet-249	13	2	to	to	ADP
admet-249	13	3	their	their	PRON
admet-249	13	4	ability	ability	NOUN
admet-249	13	5	to	to	PART
admet-249	13	6	act	act	VERB
admet-249	13	7	as	as	ADP
admet-249	13	8	chelate	chelate	NOUN
admet-249	13	9	ligands	ligand	NOUN
admet-249	13	10	and	and	CCONJ
admet-249	13	11	stabilise	stabilise	VERB
admet-249	13	12	metal	metal	NOUN
admet-249	13	13	ions	ion	NOUN
admet-249	13	14	in	in	ADP
admet-249	13	15	different	different	ADJ
admet-249	13	16	oxidation	oxidation	NOUN
admet-249	13	17	states	state	NOUN
admet-249	13	18	,	,	PUNCT
admet-249	13	19	carbohydrazide	carbohydrazide	PROPN
admet-249	13	20	schiff	schiff	NOUN
admet-249	13	21	bases	basis	NOUN
admet-249	13	22	have	have	AUX
admet-249	13	23	also	also	ADV
admet-249	13	24	found	find	VERB
admet-249	13	25	applications	application	NOUN
admet-249	13	26	as	as	ADP
admet-249	13	27	multitopic	multitopic	ADJ
admet-249	13	28	ligands	ligand	NOUN
admet-249	13	29	for	for	ADP
admet-249	13	30	the	the	DET
admet-249	13	31	targeted	target	VERB
admet-249	13	32	construction	construction	NOUN
admet-249	13	33	of	of	ADP
admet-249	13	34	bioactive	bioactive	ADJ
admet-249	13	35	coordination	coordination	NOUN
admet-249	13	36	systems	system	NOUN
admet-249	13	37	[	[	X
admet-249	13	38	7,8	7,8	NUM
admet-249	13	39	]	]	PUNCT
admet-249	13	40	.	.	PUNCT
admet-249	14	1	these	these	DET
admet-249	14	2	compounds	compound	NOUN
admet-249	14	3	can	can	AUX
admet-249	14	4	easily	easily	ADV
admet-249	14	5	be	be	AUX
admet-249	14	6	prepared	prepare	VERB
admet-249	14	7	by	by	ADP
admet-249	14	8	the	the	DET
admet-249	14	9	condensation	condensation	NOUN
admet-249	14	10	reaction	reaction	NOUN
admet-249	14	11	between	between	ADP
admet-249	14	12	carbohydrazide	carbohydrazide	NOUN
admet-249	14	13	and	and	CCONJ
admet-249	14	14	appropriate	appropriate	ADJ
admet-249	14	15	aldehyde	aldehyde	NOUN
admet-249	14	16	or	or	CCONJ
admet-249	14	17	ketone	ketone	NOUN
admet-249	14	18	.	.	PUNCT
admet-249	15	1	the	the	DET
admet-249	15	2	condensation	condensation	NOUN
admet-249	15	3	of	of	ADP
admet-249	15	4	carbohydrazide	carbohydrazide	NOUN
admet-249	15	5	(	(	PUNCT
admet-249	15	6	i	i	NOUN
admet-249	15	7	)	)	PUNCT
admet-249	15	8	with	with	ADP
admet-249	15	9	salicylaldehyde	salicylaldehyde	PROPN
admet-249	15	10	(	(	PUNCT
admet-249	15	11	ii	ii	NOUN
admet-249	15	12	)	)	PUNCT
admet-249	15	13	yielded	yield	VERB
admet-249	15	14	a	a	DET
admet-249	15	15	mixture	mixture	NOUN
admet-249	15	16	of	of	ADP
admet-249	15	17	mono(iii	mono(iii	NOUN
admet-249	15	18	)	)	PUNCT
admet-249	15	19	and	and	CCONJ
admet-249	15	20	bis(salicylidene)carbohydrazide	bis(salicylidene)carbohydrazide	NUM
admet-249	15	21	(	(	PUNCT
admet-249	15	22	iv	iv	X
admet-249	15	23	)	)	PUNCT
admet-249	15	24	,	,	PUNCT
admet-249	15	25	as	as	SCONJ
admet-249	15	26	shown	show	VERB
admet-249	15	27	in	in	ADP
admet-249	15	28	figure	figure	NOUN
admet-249	15	29	1	1	NUM
admet-249	15	30	[	[	X
admet-249	15	31	9,10	9,10	NUM
admet-249	15	32	]	]	X
admet-249	15	33	.	.	PUNCT
admet-249	16	1	http://www.pub.iapchem.org/ojs/index.php/admet/index	http://www.pub.iapchem.org/ojs/index.php/admet/index	NOUN
admet-249	16	2	mailto:ihabinovec@chem.pmf.hr	mailto:ihabinovec@chem.pmf.hr	PROPN
admet-249	16	3	mailto:tjednacak@chem.pmf.hr	mailto:tjednacak@chem.pmf.hr	PROPN
admet-249	16	4	mailto:pnovak@chem.pmf.hr	mailto:pnovak@chem.pmf.hr	PROPN
admet-249	16	5	admet	admet	PROPN
admet-249	16	6	&	&	CCONJ
admet-249	16	7	dmpk	dmpk	PROPN
admet-249	16	8	3(4	3(4	NUM
admet-249	16	9	)	)	PUNCT
admet-249	16	10	(	(	PUNCT
admet-249	16	11	2015	2015	NUM
admet-249	16	12	)	)	PUNCT
admet-249	16	13	352	352	NUM
admet-249	16	14	-	-	SYM
admet-249	16	15	358	358	NUM
admet-249	16	16	carbohydrazide	carbohydrazide	ADJ
admet-249	16	17	reaction	reaction	NOUN
admet-249	16	18	monitoring	monitoring	NOUN
admet-249	16	19	by	by	ADP
admet-249	16	20	lc	lc	PROPN
admet-249	16	21	-	-	PUNCT
admet-249	16	22	dad	dad	NOUN
admet-249	16	23	-	-	PUNCT
admet-249	16	24	spe	spe	PROPN
admet-249	16	25	-	-	PUNCT
admet-249	16	26	nmr	nmr	NOUN
admet-249	16	27	doi	doi	NOUN
admet-249	16	28	:	:	PUNCT
admet-249	16	29	10.5599	10.5599	NUM
admet-249	16	30	/	/	SYM
admet-249	16	31	admet.3.4.249	admet.3.4.249	NOUN
admet-249	16	32	353	353	NUM
admet-249	16	33	figure	figure	NOUN
admet-249	16	34	1	1	NUM
admet-249	16	35	.	.	PUNCT
admet-249	17	1	the	the	DET
admet-249	17	2	condensation	condensation	NOUN
admet-249	17	3	reaction	reaction	NOUN
admet-249	17	4	between	between	ADP
admet-249	17	5	carbohydrazide	carbohydrazide	NOUN
admet-249	17	6	and	and	CCONJ
admet-249	17	7	salicylaldehyde	salicylaldehyde	NOUN
admet-249	17	8	.	.	PUNCT
admet-249	18	1	we	we	PRON
admet-249	18	2	have	have	AUX
admet-249	18	3	recently	recently	ADV
admet-249	18	4	reported	report	VERB
admet-249	18	5	that	that	SCONJ
admet-249	18	6	in	in	ADP
admet-249	18	7	-	-	PUNCT
admet-249	18	8	line	line	NOUN
admet-249	18	9	raman	raman	NOUN
admet-249	18	10	spectroscopy	spectroscopy	NOUN
admet-249	18	11	combined	combine	VERB
admet-249	18	12	with	with	ADP
admet-249	18	13	multivariate	multivariate	NOUN
admet-249	18	14	data	datum	NOUN
admet-249	18	15	analysis	analysis	NOUN
admet-249	18	16	could	could	AUX
admet-249	18	17	be	be	AUX
admet-249	18	18	applied	apply	VERB
admet-249	18	19	for	for	ADP
admet-249	18	20	in	in	ADP
admet-249	18	21	-	-	PUNCT
admet-249	18	22	line	line	NOUN
admet-249	18	23	monitoring	monitoring	NOUN
admet-249	18	24	of	of	ADP
admet-249	18	25	condensation	condensation	NOUN
admet-249	18	26	reaction	reaction	NOUN
admet-249	18	27	and	and	CCONJ
admet-249	18	28	for	for	ADP
admet-249	18	29	assessing	assess	VERB
admet-249	18	30	the	the	DET
admet-249	18	31	mixture	mixture	NOUN
admet-249	18	32	content	content	NOUN
admet-249	18	33	[	[	X
admet-249	18	34	11	11	NUM
admet-249	18	35	]	]	PUNCT
admet-249	18	36	.	.	PUNCT
admet-249	19	1	however	however	ADV
admet-249	19	2	,	,	PUNCT
admet-249	19	3	several	several	ADJ
admet-249	19	4	drawbacks	drawback	NOUN
admet-249	19	5	of	of	ADP
admet-249	19	6	this	this	DET
admet-249	19	7	methodology	methodology	NOUN
admet-249	19	8	,	,	PUNCT
admet-249	19	9	such	such	ADJ
admet-249	19	10	as	as	ADP
admet-249	19	11	low	low	ADJ
admet-249	19	12	sensitivity	sensitivity	NOUN
admet-249	19	13	,	,	PUNCT
admet-249	19	14	complexity	complexity	NOUN
admet-249	19	15	of	of	ADP
admet-249	19	16	the	the	DET
admet-249	19	17	reaction	reaction	NOUN
admet-249	19	18	mixture	mixture	NOUN
admet-249	19	19	,	,	PUNCT
admet-249	19	20	and	and	CCONJ
admet-249	19	21	severe	severe	ADJ
admet-249	19	22	band	band	NOUN
admet-249	19	23	overlapping	overlap	VERB
admet-249	19	24	,	,	PUNCT
admet-249	19	25	prevented	prevent	VERB
admet-249	19	26	precise	precise	ADJ
admet-249	19	27	identification	identification	NOUN
admet-249	19	28	of	of	ADP
admet-249	19	29	the	the	DET
admet-249	19	30	compounds	compound	NOUN
admet-249	19	31	in	in	ADP
admet-249	19	32	the	the	DET
admet-249	19	33	reaction	reaction	NOUN
admet-249	19	34	mixture	mixture	NOUN
admet-249	19	35	and	and	CCONJ
admet-249	19	36	determination	determination	NOUN
admet-249	19	37	of	of	ADP
admet-249	19	38	the	the	DET
admet-249	19	39	reaction	reaction	NOUN
admet-249	19	40	endpoints	endpoint	NOUN
admet-249	19	41	directly	directly	ADV
admet-249	19	42	from	from	ADP
admet-249	19	43	the	the	DET
admet-249	19	44	in	in	ADP
admet-249	19	45	-	-	PUNCT
admet-249	19	46	line	line	NOUN
admet-249	19	47	spectra	spectra	NOUN
admet-249	19	48	.	.	PUNCT
admet-249	20	1	in	in	ADP
admet-249	20	2	order	order	NOUN
admet-249	20	3	to	to	PART
admet-249	20	4	resolve	resolve	VERB
admet-249	20	5	these	these	DET
admet-249	20	6	issues	issue	NOUN
admet-249	20	7	,	,	PUNCT
admet-249	20	8	we	we	PRON
admet-249	20	9	employed	employ	VERB
admet-249	20	10	here	here	ADV
admet-249	20	11	an	an	DET
admet-249	20	12	approach	approach	NOUN
admet-249	20	13	based	base	VERB
admet-249	20	14	on	on	ADP
admet-249	20	15	the	the	DET
admet-249	20	16	hyphenated	hyphenate	VERB
admet-249	20	17	system	system	NOUN
admet-249	20	18	comprising	comprising	NOUN
admet-249	20	19	of	of	ADP
admet-249	20	20	high	high	ADJ
admet-249	20	21	performance	performance	NOUN
admet-249	20	22	liquid	liquid	NOUN
admet-249	20	23	chromatography	chromatography	NOUN
admet-249	20	24	with	with	ADP
admet-249	20	25	diode	diode	NOUN
admet-249	20	26	array	array	NOUN
admet-249	20	27	detection	detection	NOUN
admet-249	20	28	(	(	PUNCT
admet-249	20	29	lc	lc	NOUN
admet-249	20	30	-	-	PUNCT
admet-249	20	31	dad	dad	NOUN
admet-249	20	32	)	)	PUNCT
admet-249	20	33	,	,	PUNCT
admet-249	20	34	solid	solid	ADJ
admet-249	20	35	phase	phase	NOUN
admet-249	20	36	extraction	extraction	NOUN
admet-249	20	37	(	(	PUNCT
admet-249	20	38	spe	spe	PROPN
admet-249	20	39	)	)	PUNCT
admet-249	20	40	and	and	CCONJ
admet-249	20	41	nuclear	nuclear	ADJ
admet-249	20	42	magnetic	magnetic	ADJ
admet-249	20	43	resonance	resonance	NOUN
admet-249	20	44	spectroscopy	spectroscopy	NOUN
admet-249	20	45	equipped	equip	VERB
admet-249	20	46	with	with	ADP
admet-249	20	47	a	a	DET
admet-249	20	48	cryogenically	cryogenically	ADV
admet-249	20	49	cooled	cool	VERB
admet-249	20	50	probe	probe	NOUN
admet-249	20	51	(	(	PUNCT
admet-249	20	52	cryo	cryo	PROPN
admet-249	20	53	nmr	nmr	NOUN
admet-249	20	54	)	)	PUNCT
admet-249	20	55	.	.	PUNCT
admet-249	21	1	this	this	DET
admet-249	21	2	lcdad	lcdad	PROPN
admet-249	21	3	-	-	PUNCT
admet-249	21	4	spe	spe	NOUN
admet-249	21	5	-	-	PUNCT
admet-249	21	6	nmr	nmr	NOUN
admet-249	21	7	setup	setup	NOUN
admet-249	21	8	represents	represent	VERB
admet-249	21	9	a	a	DET
admet-249	21	10	state	state	NOUN
admet-249	21	11	-	-	PUNCT
admet-249	21	12	of	of	ADP
admet-249	21	13	-	-	PUNCT
admet-249	21	14	the	the	DET
admet-249	21	15	-	-	PUNCT
admet-249	21	16	art	art	NOUN
admet-249	21	17	technology	technology	NOUN
admet-249	21	18	for	for	ADP
admet-249	21	19	rapid	rapid	ADJ
admet-249	21	20	and	and	CCONJ
admet-249	21	21	accurate	accurate	ADJ
admet-249	21	22	mixture	mixture	NOUN
admet-249	21	23	analysis	analysis	NOUN
admet-249	21	24	.	.	PUNCT
admet-249	22	1	the	the	DET
admet-249	22	2	coupling	coupling	NOUN
admet-249	22	3	of	of	ADP
admet-249	22	4	hplc	hplc	PROPN
admet-249	22	5	with	with	ADP
admet-249	22	6	nmr	nmr	NOUN
admet-249	22	7	spectroscopy	spectroscopy	NOUN
admet-249	22	8	has	have	AUX
admet-249	22	9	become	become	VERB
admet-249	22	10	one	one	NUM
admet-249	22	11	of	of	ADP
admet-249	22	12	the	the	DET
admet-249	22	13	most	most	ADV
admet-249	22	14	efficient	efficient	ADJ
admet-249	22	15	and	and	CCONJ
admet-249	22	16	powerful	powerful	ADJ
admet-249	22	17	analytical	analytical	ADJ
admet-249	22	18	technique	technique	NOUN
admet-249	22	19	to	to	PART
admet-249	22	20	analyse	analyse	VERB
admet-249	22	21	complex	complex	ADJ
admet-249	22	22	mixtures	mixture	NOUN
admet-249	22	23	.	.	PUNCT
admet-249	23	1	identification	identification	NOUN
admet-249	23	2	and	and	CCONJ
admet-249	23	3	structural	structural	ADJ
admet-249	23	4	characterization	characterization	NOUN
admet-249	23	5	of	of	ADP
admet-249	23	6	compounds	compound	NOUN
admet-249	23	7	in	in	ADP
admet-249	23	8	a	a	DET
admet-249	23	9	mixture	mixture	NOUN
admet-249	23	10	without	without	ADP
admet-249	23	11	their	their	PRON
admet-249	23	12	physical	physical	ADJ
admet-249	23	13	separation	separation	NOUN
admet-249	23	14	has	have	AUX
admet-249	23	15	long	long	ADV
admet-249	23	16	been	be	AUX
admet-249	23	17	a	a	DET
admet-249	23	18	dream	dream	NOUN
admet-249	23	19	of	of	ADP
admet-249	23	20	analytical	analytical	ADJ
admet-249	23	21	chemists	chemist	NOUN
admet-249	23	22	.	.	PUNCT
admet-249	24	1	lc	lc	NOUN
admet-249	24	2	-	-	PUNCT
admet-249	24	3	nmr	nmr	NOUN
admet-249	24	4	hyphenation	hyphenation	PROPN
admet-249	24	5	gives	give	VERB
admet-249	24	6	a	a	DET
admet-249	24	7	wealth	wealth	NOUN
admet-249	24	8	of	of	ADP
admet-249	24	9	structural	structural	ADJ
admet-249	24	10	information	information	NOUN
admet-249	24	11	on	on	ADP
admet-249	24	12	small	small	ADJ
admet-249	24	13	quantities	quantity	NOUN
admet-249	24	14	of	of	ADP
admet-249	24	15	substances	substance	NOUN
admet-249	24	16	without	without	ADP
admet-249	24	17	the	the	DET
admet-249	24	18	necessity	necessity	NOUN
admet-249	24	19	of	of	ADP
admet-249	24	20	their	their	PRON
admet-249	24	21	isolation	isolation	NOUN
admet-249	24	22	and	and	CCONJ
admet-249	24	23	purification	purification	NOUN
admet-249	24	24	[	[	X
admet-249	24	25	12	12	NUM
admet-249	24	26	-	-	SYM
admet-249	24	27	16	16	NUM
admet-249	24	28	]	]	PUNCT
admet-249	24	29	.	.	PUNCT
admet-249	25	1	a	a	DET
admet-249	25	2	further	further	ADJ
admet-249	25	3	coupling	coupling	NOUN
admet-249	25	4	of	of	ADP
admet-249	25	5	lc	lc	NOUN
admet-249	25	6	-	-	PUNCT
admet-249	25	7	nmr	nmr	NOUN
admet-249	25	8	to	to	PART
admet-249	25	9	spe	spe	PROPN
admet-249	25	10	has	have	AUX
admet-249	25	11	considerably	considerably	ADV
admet-249	25	12	improved	improve	VERB
admet-249	25	13	the	the	DET
admet-249	25	14	sensitivity	sensitivity	NOUN
admet-249	25	15	of	of	ADP
admet-249	25	16	this	this	DET
admet-249	25	17	technique	technique	NOUN
admet-249	25	18	by	by	ADP
admet-249	25	19	post	post	NOUN
admet-249	25	20	column	column	NOUN
admet-249	25	21	peak	peak	NOUN
admet-249	25	22	trapping	trap	VERB
admet-249	25	23	onto	onto	ADP
admet-249	25	24	the	the	DET
admet-249	25	25	spe	spe	ADJ
admet-249	25	26	cartridges	cartridge	NOUN
admet-249	25	27	enabling	enable	VERB
admet-249	25	28	the	the	DET
admet-249	25	29	separate	separate	ADJ
admet-249	25	30	compounds	compound	NOUN
admet-249	25	31	to	to	PART
admet-249	25	32	be	be	AUX
admet-249	25	33	concentrated	concentrate	VERB
admet-249	25	34	and	and	CCONJ
admet-249	25	35	eluted	elute	VERB
admet-249	25	36	fully	fully	ADV
admet-249	25	37	with	with	ADP
admet-249	25	38	deuterated	deuterate	VERB
admet-249	25	39	solvents	solvent	NOUN
admet-249	25	40	.	.	PUNCT
admet-249	26	1	lc	lc	NOUN
admet-249	26	2	-	-	PUNCT
admet-249	26	3	spe	spe	NOUN
admet-249	26	4	-	-	PUNCT
admet-249	26	5	nmr	nmr	NOUN
admet-249	26	6	is	be	AUX
admet-249	26	7	now	now	ADV
admet-249	26	8	widely	widely	ADV
admet-249	26	9	accepted	accept	VERB
admet-249	26	10	tool	tool	NOUN
admet-249	26	11	for	for	ADP
admet-249	26	12	dereplication	dereplication	NOUN
admet-249	26	13	and	and	CCONJ
admet-249	26	14	discovery	discovery	NOUN
admet-249	26	15	of	of	ADP
admet-249	26	16	natural	natural	ADJ
admet-249	26	17	products	product	NOUN
admet-249	26	18	from	from	ADP
admet-249	26	19	complex	complex	ADJ
admet-249	26	20	mixtures	mixture	NOUN
admet-249	26	21	of	of	ADP
admet-249	26	22	plants	plant	NOUN
admet-249	26	23	,	,	PUNCT
admet-249	26	24	metabolites	metabolite	NOUN
admet-249	26	25	,	,	PUNCT
admet-249	26	26	drug	drug	NOUN
admet-249	26	27	impurity	impurity	NOUN
admet-249	26	28	profiling	profiling	NOUN
admet-249	26	29	and	and	CCONJ
admet-249	26	30	environmental	environmental	ADJ
admet-249	26	31	analysis	analysis	NOUN
admet-249	26	32	[	[	X
admet-249	26	33	17	17	NUM
admet-249	26	34	-	-	SYM
admet-249	26	35	21	21	NUM
admet-249	26	36	]	]	PUNCT
admet-249	26	37	.	.	PUNCT
admet-249	27	1	on	on	ADP
admet-249	27	2	the	the	DET
admet-249	27	3	other	other	ADJ
admet-249	27	4	hand	hand	NOUN
admet-249	27	5	,	,	PUNCT
admet-249	27	6	it	it	PRON
admet-249	27	7	has	have	AUX
admet-249	27	8	been	be	AUX
admet-249	27	9	less	less	ADV
admet-249	27	10	frequently	frequently	ADV
admet-249	27	11	used	use	VERB
admet-249	27	12	to	to	PART
admet-249	27	13	monitor	monitor	VERB
admet-249	27	14	chemical	chemical	ADJ
admet-249	27	15	reaction	reaction	NOUN
admet-249	27	16	products	product	NOUN
admet-249	28	1	[	[	X
admet-249	28	2	22,23	22,23	NOUN
admet-249	28	3	]	]	PUNCT
admet-249	28	4	.	.	PUNCT
admet-249	29	1	hence	hence	ADV
admet-249	29	2	,	,	PUNCT
admet-249	29	3	in	in	ADP
admet-249	29	4	the	the	DET
admet-249	29	5	present	present	ADJ
admet-249	29	6	work	work	NOUN
admet-249	29	7	we	we	PRON
admet-249	29	8	applied	apply	VERB
admet-249	29	9	this	this	DET
admet-249	29	10	hyphenated	hyphenate	VERB
admet-249	29	11	method	method	NOUN
admet-249	29	12	to	to	PART
admet-249	29	13	analyse	analyse	VERB
admet-249	29	14	carbohydrazide	carbohydrazide	NOUN
admet-249	29	15	condensation	condensation	NOUN
admet-249	29	16	reaction	reaction	NOUN
admet-249	29	17	.	.	PUNCT
admet-249	30	1	oneand	oneand	CCONJ
admet-249	30	2	two	two	NUM
admet-249	30	3	-	-	PUNCT
admet-249	30	4	dimensional	dimensional	ADJ
admet-249	30	5	nmr	nmr	NOUN
admet-249	30	6	experiments	experiment	NOUN
admet-249	30	7	with	with	ADP
admet-249	30	8	a	a	DET
admet-249	30	9	noesy	noesy	NOUN
admet-249	30	10	-	-	PUNCT
admet-249	30	11	type	type	NOUN
admet-249	30	12	double	double	ADJ
admet-249	30	13	presaturation	presaturation	NOUN
admet-249	30	14	for	for	ADP
admet-249	30	15	suppressing	suppress	VERB
admet-249	30	16	acetonitirile	acetonitirile	ADJ
admet-249	30	17	and	and	CCONJ
admet-249	30	18	water	water	NOUN
admet-249	30	19	resonances	resonance	NOUN
admet-249	30	20	will	will	AUX
admet-249	30	21	be	be	AUX
admet-249	30	22	used	use	VERB
admet-249	30	23	for	for	ADP
admet-249	30	24	structure	structure	NOUN
admet-249	30	25	elucidation	elucidation	NOUN
admet-249	30	26	of	of	ADP
admet-249	30	27	mixture	mixture	NOUN
admet-249	30	28	components	component	NOUN
admet-249	30	29	.	.	PUNCT
admet-249	31	1	experimental	experimental	ADJ
admet-249	31	2	chemicals	chemical	NOUN
admet-249	31	3	salicylaldehyde	salicylaldehyde	NOUN
admet-249	31	4	(	(	PUNCT
admet-249	31	5	min	min	NOUN
admet-249	31	6	.	.	PROPN
admet-249	31	7	98	98	NUM
admet-249	31	8	%	%	NOUN
admet-249	31	9	)	)	PUNCT
admet-249	31	10	and	and	CCONJ
admet-249	31	11	carbohydrazide	carbohydrazide	NOUN
admet-249	31	12	(	(	PUNCT
admet-249	31	13	min	min	NOUN
admet-249	31	14	.	.	PROPN
admet-249	31	15	98	98	NUM
admet-249	31	16	%	%	NOUN
admet-249	31	17	)	)	PUNCT
admet-249	31	18	were	be	AUX
admet-249	31	19	purchased	purchase	VERB
admet-249	31	20	from	from	ADP
admet-249	31	21	sigma	sigma	PROPN
admet-249	31	22	-	-	PUNCT
admet-249	31	23	aldrich	aldrich	PROPN
admet-249	31	24	(	(	PUNCT
admet-249	31	25	mo	mo	PROPN
admet-249	31	26	,	,	PUNCT
admet-249	31	27	usa	usa	PROPN
admet-249	31	28	)	)	PUNCT
admet-249	31	29	.	.	PUNCT
admet-249	32	1	piperidine	piperidine	NOUN
admet-249	32	2	(	(	PUNCT
admet-249	32	3	min	min	NOUN
admet-249	32	4	.	.	PROPN
admet-249	32	5	99	99	NUM
admet-249	32	6	%	%	NOUN
admet-249	32	7	)	)	PUNCT
admet-249	32	8	was	be	AUX
admet-249	32	9	purchased	purchase	VERB
admet-249	32	10	from	from	ADP
admet-249	32	11	acros	acros	PROPN
admet-249	32	12	organics	organic	NOUN
admet-249	32	13	(	(	PUNCT
admet-249	32	14	nj	nj	PROPN
admet-249	32	15	,	,	PUNCT
admet-249	32	16	usa	usa	PROPN
admet-249	32	17	)	)	PUNCT
admet-249	32	18	.	.	PUNCT
admet-249	33	1	methanol	methanol	NOUN
admet-249	33	2	(	(	PUNCT
admet-249	33	3	min	min	NOUN
admet-249	33	4	.	.	PROPN
admet-249	33	5	99.95	99.95	NUM
admet-249	33	6	%	%	NOUN
admet-249	33	7	)	)	PUNCT
admet-249	33	8	was	be	AUX
admet-249	33	9	obtained	obtain	VERB
admet-249	33	10	from	from	ADP
admet-249	33	11	carl	carl	PROPN
admet-249	33	12	roth	roth	PROPN
admet-249	33	13	gmbh	gmbh	PROPN
admet-249	33	14	(	(	PUNCT
admet-249	33	15	karlsruhe	karlsruhe	PROPN
admet-249	33	16	,	,	PUNCT
admet-249	33	17	germany	germany	PROPN
admet-249	33	18	)	)	PUNCT
admet-249	33	19	.	.	PUNCT
admet-249	34	1	acetonitrile	acetonitrile	NOUN
admet-249	34	2	(	(	PUNCT
admet-249	34	3	hplc	hplc	NOUN
admet-249	34	4	grade	grade	NOUN
admet-249	34	5	)	)	PUNCT
admet-249	34	6	was	be	AUX
admet-249	34	7	purchased	purchase	VERB
admet-249	34	8	from	from	ADP
admet-249	34	9	j.	j.	PROPN
admet-249	34	10	t.	t.	PROPN
admet-249	34	11	baker	baker	PROPN
admet-249	34	12	(	(	PUNCT
admet-249	34	13	pa	pa	PROPN
admet-249	34	14	,	,	PUNCT
admet-249	34	15	usa	usa	PROPN
admet-249	34	16	)	)	PUNCT
admet-249	34	17	and	and	CCONJ
admet-249	34	18	potassium	potassium	NOUN
admet-249	34	19	dihydrogen	dihydrogen	NOUN
admet-249	34	20	phosphate	phosphate	NOUN
admet-249	34	21	(	(	PUNCT
admet-249	34	22	for	for	ADP
admet-249	34	23	chromatography	chromatography	NOUN
admet-249	34	24	)	)	PUNCT
admet-249	34	25	was	be	AUX
admet-249	34	26	obtained	obtain	VERB
admet-249	34	27	from	from	ADP
admet-249	34	28	kemika	kemika	PROPN
admet-249	34	29	habinovec	habinovec	PROPN
admet-249	34	30	et	et	PROPN
admet-249	34	31	al	al	PROPN
admet-249	34	32	.	.	PROPN
admet-249	34	33	admet	admet	PROPN
admet-249	34	34	&	&	CCONJ
admet-249	34	35	dmpk	dmpk	PROPN
admet-249	34	36	3(4	3(4	NUM
admet-249	34	37	)	)	PUNCT
admet-249	34	38	(	(	PUNCT
admet-249	34	39	2015	2015	NUM
admet-249	34	40	)	)	PUNCT
admet-249	34	41	352	352	NUM
admet-249	34	42	-	-	SYM
admet-249	34	43	358	358	NUM
admet-249	34	44	354	354	NUM
admet-249	34	45	(	(	PUNCT
admet-249	34	46	zagreb	zagreb	PROPN
admet-249	34	47	,	,	PUNCT
admet-249	34	48	croatia	croatia	PROPN
admet-249	34	49	)	)	PUNCT
admet-249	34	50	.	.	PUNCT
admet-249	35	1	acetonitrile	acetonitrile	NOUN
admet-249	35	2	-	-	PUNCT
admet-249	35	3	d3	d3	PROPN
admet-249	35	4	(	(	PUNCT
admet-249	35	5	d	d	PROPN
admet-249	35	6	,	,	PUNCT
admet-249	35	7	99.8	99.8	NUM
admet-249	35	8	%	%	NOUN
admet-249	35	9	)	)	PUNCT
admet-249	35	10	was	be	AUX
admet-249	35	11	purchased	purchase	VERB
admet-249	35	12	from	from	ADP
admet-249	35	13	cambridge	cambridge	PROPN
admet-249	35	14	isotope	isotope	NOUN
admet-249	35	15	laboratories	laboratory	NOUN
admet-249	35	16	,	,	PUNCT
admet-249	35	17	inc	inc	PROPN
admet-249	35	18	.	.	PROPN
admet-249	35	19	(	(	PUNCT
admet-249	35	20	ma	ma	PROPN
admet-249	35	21	,	,	PUNCT
admet-249	35	22	usa	usa	PROPN
admet-249	35	23	)	)	PUNCT
admet-249	35	24	.	.	PUNCT
admet-249	36	1	synthesis	synthesis	NOUN
admet-249	36	2	carbohydrazide	carbohydrazide	NOUN
admet-249	36	3	(	(	PUNCT
admet-249	36	4	0.60	0.60	NUM
admet-249	36	5	g	g	NOUN
admet-249	36	6	,	,	PUNCT
admet-249	36	7	6.67	6.67	NUM
admet-249	36	8	mmol	mmol	NOUN
admet-249	36	9	)	)	PUNCT
admet-249	36	10	was	be	AUX
admet-249	36	11	gradually	gradually	ADV
admet-249	36	12	dissolved	dissolve	VERB
admet-249	36	13	in	in	ADP
admet-249	36	14	40	40	NUM
admet-249	36	15	ml	ml	NOUN
admet-249	36	16	of	of	ADP
admet-249	36	17	methanol	methanol	NOUN
admet-249	36	18	.	.	PUNCT
admet-249	37	1	after	after	ADP
admet-249	37	2	the	the	DET
admet-249	37	3	addition	addition	NOUN
admet-249	37	4	of	of	ADP
admet-249	37	5	salicylaldehyde	salicylaldehyde	PROPN
admet-249	37	6	(	(	PUNCT
admet-249	37	7	0.71	0.71	NUM
admet-249	37	8	ml	ml	NOUN
admet-249	37	9	,	,	PUNCT
admet-249	37	10	6.67	6.67	NUM
admet-249	37	11	mmol	mmol	NOUN
admet-249	37	12	)	)	PUNCT
admet-249	37	13	and	and	CCONJ
admet-249	37	14	a	a	DET
admet-249	37	15	few	few	ADJ
admet-249	37	16	drops	drop	NOUN
admet-249	37	17	of	of	ADP
admet-249	37	18	piperidine	piperidine	NOUN
admet-249	37	19	,	,	PUNCT
admet-249	37	20	the	the	DET
admet-249	37	21	reaction	reaction	NOUN
admet-249	37	22	mixture	mixture	NOUN
admet-249	37	23	was	be	AUX
admet-249	37	24	heated	heat	VERB
admet-249	37	25	at	at	ADP
admet-249	37	26	55	55	NUM
admet-249	37	27	°	°	ADP
admet-249	37	28	c	c	NOUN
admet-249	37	29	and	and	CCONJ
admet-249	37	30	stirred	stir	VERB
admet-249	37	31	under	under	ADP
admet-249	37	32	reflux	reflux	NOUN
admet-249	37	33	for	for	ADP
admet-249	37	34	40	40	NUM
admet-249	37	35	min	min	NOUN
admet-249	38	1	[	[	X
admet-249	38	2	9	9	NUM
admet-249	38	3	]	]	PUNCT
admet-249	38	4	.	.	PUNCT
admet-249	39	1	during	during	ADP
admet-249	39	2	heating	heating	NOUN
admet-249	39	3	,	,	PUNCT
admet-249	39	4	a	a	DET
admet-249	39	5	white	white	ADJ
admet-249	39	6	crystalline	crystalline	NOUN
admet-249	39	7	product	product	NOUN
admet-249	39	8	started	start	VERB
admet-249	39	9	to	to	PART
admet-249	39	10	precipitate	precipitate	VERB
admet-249	39	11	.	.	PUNCT
admet-249	40	1	the	the	DET
admet-249	40	2	product	product	NOUN
admet-249	40	3	was	be	AUX
admet-249	40	4	filtered	filter	VERB
admet-249	40	5	off	off	ADP
admet-249	40	6	,	,	PUNCT
admet-249	40	7	washed	wash	VERB
admet-249	40	8	with	with	ADP
admet-249	40	9	a	a	DET
admet-249	40	10	small	small	ADJ
admet-249	40	11	amount	amount	NOUN
admet-249	40	12	of	of	ADP
admet-249	40	13	cold	cold	ADJ
admet-249	40	14	methanol	methanol	NOUN
admet-249	40	15	and	and	CCONJ
admet-249	40	16	dried	dry	VERB
admet-249	40	17	in	in	ADP
admet-249	40	18	air	air	NOUN
admet-249	40	19	.	.	PUNCT
admet-249	41	1	lc	lc	NOUN
admet-249	41	2	-	-	PUNCT
admet-249	41	3	spe	spe	PROPN
admet-249	41	4	analysis	analysis	NOUN
admet-249	41	5	an	an	DET
admet-249	41	6	agilent	agilent	PROPN
admet-249	41	7	1260	1260	NUM
admet-249	41	8	infinity	infinity	NOUN
admet-249	41	9	hplc	hplc	NOUN
admet-249	41	10	system	system	NOUN
admet-249	41	11	equipped	equip	VERB
admet-249	41	12	with	with	ADP
admet-249	41	13	quaternary	quaternary	ADJ
admet-249	41	14	pump	pump	NOUN
admet-249	41	15	,	,	PUNCT
admet-249	41	16	an	an	DET
admet-249	41	17	autosampler	autosampler	NOUN
admet-249	41	18	,	,	PUNCT
admet-249	41	19	thermostatted	thermostatte	VERB
admet-249	41	20	column	column	NOUN
admet-249	41	21	compartment	compartment	NOUN
admet-249	41	22	and	and	CCONJ
admet-249	41	23	dad	dad	NOUN
admet-249	41	24	detector	detector	NOUN
admet-249	41	25	was	be	AUX
admet-249	41	26	used	use	VERB
admet-249	41	27	for	for	ADP
admet-249	41	28	chromatographic	chromatographic	ADJ
admet-249	41	29	separation	separation	NOUN
admet-249	41	30	prior	prior	ADV
admet-249	41	31	to	to	ADP
admet-249	41	32	post	post	ADJ
admet-249	41	33	-	-	ADJ
admet-249	41	34	column	column	ADJ
admet-249	41	35	solid	solid	ADJ
admet-249	41	36	-	-	PUNCT
admet-249	41	37	phase	phase	NOUN
admet-249	41	38	extraction	extraction	NOUN
admet-249	41	39	.	.	PUNCT
admet-249	42	1	separation	separation	NOUN
admet-249	42	2	was	be	AUX
admet-249	42	3	performed	perform	VERB
admet-249	42	4	on	on	ADP
admet-249	42	5	an	an	DET
admet-249	42	6	agilent	agilent	PROPN
admet-249	42	7	poroshell	poroshell	PROPN
admet-249	42	8	120	120	NUM
admet-249	42	9	c18	c18	NOUN
admet-249	42	10	column	column	NOUN
admet-249	42	11	(	(	PUNCT
admet-249	42	12	250	250	NUM
admet-249	42	13	mm	mm	NOUN
admet-249	42	14	x	x	SYM
admet-249	42	15	4.6	4.6	NUM
admet-249	42	16	mm	mm	NOUN
admet-249	42	17	)	)	PUNCT
admet-249	42	18	with	with	ADP
admet-249	42	19	4	4	NUM
admet-249	42	20	μm	μm	NOUN
admet-249	42	21	particle	particle	NOUN
admet-249	42	22	size	size	NOUN
admet-249	42	23	in	in	ADP
admet-249	42	24	analytical	analytical	ADJ
admet-249	42	25	mode	mode	NOUN
admet-249	42	26	.	.	PUNCT
admet-249	43	1	injection	injection	NOUN
admet-249	43	2	volume	volume	NOUN
admet-249	43	3	was	be	AUX
admet-249	43	4	25	25	NUM
admet-249	43	5	μl	μl	ADP
admet-249	43	6	and	and	CCONJ
admet-249	43	7	the	the	DET
admet-249	43	8	flow	flow	NOUN
admet-249	43	9	rate	rate	NOUN
admet-249	43	10	was	be	AUX
admet-249	43	11	1.0	1.0	NUM
admet-249	43	12	ml	ml	NOUN
admet-249	43	13	min	min	PROPN
admet-249	43	14	–	–	PUNCT
admet-249	43	15	1	1	NUM
admet-249	43	16	.	.	PUNCT
admet-249	44	1	elution	elution	NOUN
admet-249	44	2	was	be	AUX
admet-249	44	3	isocratic	isocratic	ADJ
admet-249	44	4	using	use	VERB
admet-249	44	5	a	a	DET
admet-249	44	6	mobile	mobile	ADJ
admet-249	44	7	phase	phase	NOUN
admet-249	44	8	consisting	consist	VERB
admet-249	44	9	of	of	ADP
admet-249	44	10	50	50	NUM
admet-249	44	11	%	%	NOUN
admet-249	44	12	acetonitrile	acetonitrile	NOUN
admet-249	44	13	and	and	CCONJ
admet-249	44	14	50	50	NUM
admet-249	44	15	%	%	NOUN
admet-249	44	16	phosphate	phosphate	NOUN
admet-249	44	17	buffer	buffer	NOUN
admet-249	44	18	(	(	PUNCT
admet-249	44	19	ph	ph	NOUN
admet-249	44	20	7	7	NUM
admet-249	44	21	)	)	PUNCT
admet-249	44	22	at	at	ADP
admet-249	44	23	298	298	NUM
admet-249	44	24	k	k	NOUN
admet-249	44	25	over	over	ADP
admet-249	44	26	10	10	NUM
admet-249	44	27	min	min	NOUN
admet-249	44	28	.	.	PUNCT
admet-249	45	1	the	the	DET
admet-249	45	2	automatic	automatic	ADJ
admet-249	45	3	post	post	ADJ
admet-249	45	4	-	-	ADJ
admet-249	45	5	column	column	ADJ
admet-249	45	6	spe	spe	NOUN
admet-249	45	7	was	be	AUX
admet-249	45	8	performed	perform	VERB
admet-249	45	9	on	on	ADP
admet-249	45	10	a	a	DET
admet-249	45	11	prospekt	prospekt	NOUN
admet-249	45	12	2	2	NUM
admet-249	45	13	lcspe	lcspe	ADJ
admet-249	45	14	-	-	PUNCT
admet-249	45	15	nmr	nmr	NOUN
admet-249	45	16	interface	interface	NOUN
admet-249	45	17	(	(	PUNCT
admet-249	45	18	spark	spark	NOUN
admet-249	45	19	holland	holland	PROPN
admet-249	45	20	,	,	PUNCT
admet-249	45	21	emmen	emman	NOUN
admet-249	45	22	,	,	PUNCT
admet-249	45	23	the	the	DET
admet-249	45	24	netherlands	netherlands	PROPN
admet-249	45	25	)	)	PUNCT
admet-249	45	26	.	.	PUNCT
admet-249	46	1	both	both	DET
admet-249	46	2	single	single	ADJ
admet-249	46	3	and	and	CCONJ
admet-249	46	4	multi	multi	ADJ
admet-249	46	5	-	-	ADJ
admet-249	46	6	trapping	trap	VERB
admet-249	46	7	methods	method	NOUN
admet-249	46	8	were	be	AUX
admet-249	46	9	used	use	VERB
admet-249	46	10	for	for	ADP
admet-249	46	11	the	the	DET
admet-249	46	12	spe	spe	ADJ
admet-249	46	13	pre	pre	NOUN
admet-249	46	14	-	-	NOUN
admet-249	46	15	concentration	concentration	NOUN
admet-249	46	16	.	.	PUNCT
admet-249	47	1	compounds	compound	NOUN
admet-249	47	2	from	from	ADP
admet-249	47	3	reaction	reaction	NOUN
admet-249	47	4	mixture	mixture	NOUN
admet-249	47	5	were	be	AUX
admet-249	47	6	trapped	trap	VERB
admet-249	47	7	on	on	ADP
admet-249	47	8	hysphere	hysphere	ADJ
admet-249	47	9	resin	resin	NOUN
admet-249	47	10	gp	gp	NOUN
admet-249	47	11	,	,	PUNCT
admet-249	47	12	c18	c18	NOUN
admet-249	47	13	and	and	CCONJ
admet-249	47	14	c8	c8	PROPN
admet-249	47	15	spe	spe	PROPN
admet-249	47	16	cartridges	cartridge	NOUN
admet-249	47	17	(	(	PUNCT
admet-249	47	18	10	10	NUM
admet-249	47	19	x	x	SYM
admet-249	47	20	2	2	NUM
admet-249	47	21	mm	mm	NOUN
admet-249	47	22	)	)	PUNCT
admet-249	47	23	.	.	PUNCT
admet-249	48	1	to	to	PART
admet-249	48	2	increase	increase	VERB
admet-249	48	3	the	the	DET
admet-249	48	4	retention	retention	NOUN
admet-249	48	5	of	of	ADP
admet-249	48	6	the	the	DET
admet-249	48	7	compounds	compound	NOUN
admet-249	48	8	on	on	ADP
admet-249	48	9	spe	spe	PROPN
admet-249	48	10	cartridges	cartridge	NOUN
admet-249	48	11	a	a	DET
admet-249	48	12	post	post	ADJ
admet-249	48	13	-	-	ADJ
admet-249	48	14	column	column	ADJ
admet-249	48	15	water	water	NOUN
admet-249	48	16	addition	addition	NOUN
admet-249	48	17	was	be	AUX
admet-249	48	18	performed	perform	VERB
admet-249	48	19	with	with	ADP
admet-249	48	20	a	a	DET
admet-249	48	21	flow	flow	NOUN
admet-249	48	22	rate	rate	NOUN
admet-249	48	23	of	of	ADP
admet-249	48	24	3.0	3.0	NUM
admet-249	48	25	ml	ml	NOUN
admet-249	48	26	min–1	min–1	NOUN
admet-249	48	27	using	use	VERB
admet-249	48	28	the	the	DET
admet-249	48	29	knauer	knauer	NOUN
admet-249	48	30	k-120	k-120	PROPN
admet-249	48	31	hplc	hplc	PROPN
admet-249	48	32	pump	pump	PROPN
admet-249	48	33	(	(	PUNCT
admet-249	48	34	knauer	knauer	PROPN
admet-249	48	35	,	,	PUNCT
admet-249	48	36	berlin	berlin	PROPN
admet-249	48	37	,	,	PUNCT
admet-249	48	38	germany	germany	PROPN
admet-249	48	39	)	)	PUNCT
admet-249	48	40	.	.	PUNCT
admet-249	49	1	after	after	SCONJ
admet-249	49	2	the	the	DET
admet-249	49	3	cartridges	cartridge	NOUN
admet-249	49	4	were	be	AUX
admet-249	49	5	dried	dry	VERB
admet-249	49	6	with	with	ADP
admet-249	49	7	nitrogen	nitrogen	NOUN
admet-249	49	8	gas	gas	NOUN
admet-249	49	9	for	for	ADP
admet-249	49	10	59	59	NUM
admet-249	49	11	min	min	NOUN
admet-249	49	12	,	,	PUNCT
admet-249	49	13	compounds	compound	NOUN
admet-249	49	14	were	be	AUX
admet-249	49	15	eluted	elute	VERB
admet-249	49	16	with	with	ADP
admet-249	49	17	336	336	NUM
admet-249	49	18	μl	μl	ADP
admet-249	49	19	of	of	ADP
admet-249	49	20	deuterated	deuterated	ADJ
admet-249	49	21	acetonitrile	acetonitrile	NOUN
admet-249	49	22	into	into	ADP
admet-249	49	23	the	the	DET
admet-249	49	24	3	3	NUM
admet-249	49	25	mm	mm	PROPN
admet-249	49	26	nmr	nmr	NOUN
admet-249	49	27	tubes	tube	NOUN
admet-249	49	28	.	.	PUNCT
admet-249	50	1	nmr	nmr	NOUN
admet-249	50	2	spectroscopy	spectroscopy	VERB
admet-249	50	3	nmr	nmr	NOUN
admet-249	50	4	spectra	spectra	NOUN
admet-249	50	5	with	with	ADP
admet-249	50	6	noesy	noesy	NOUN
admet-249	50	7	-	-	PUNCT
admet-249	50	8	type	type	NOUN
admet-249	50	9	solvent	solvent	NOUN
admet-249	50	10	suppression	suppression	NOUN
admet-249	50	11	module	module	NOUN
admet-249	50	12	were	be	AUX
admet-249	50	13	recorded	record	VERB
admet-249	50	14	on	on	ADP
admet-249	50	15	bruker	bruker	PROPN
admet-249	50	16	avance	avance	PROPN
admet-249	50	17	iii	iii	PROPN
admet-249	50	18	hd	hd	PROPN
admet-249	50	19	400	400	NUM
admet-249	50	20	spectrometer	spectrometer	NOUN
admet-249	50	21	operating	operate	VERB
admet-249	50	22	at	at	ADP
admet-249	50	23	400	400	NUM
admet-249	50	24	mhz	mhz	NOUN
admet-249	50	25	equipped	equip	VERB
admet-249	50	26	with	with	ADP
admet-249	50	27	a	a	DET
admet-249	50	28	broadband	broadband	NOUN
admet-249	50	29	observed	observe	VERB
admet-249	50	30	(	(	PUNCT
admet-249	50	31	bbo	bbo	NOUN
admet-249	50	32	)	)	PUNCT
admet-249	50	33	5	5	NUM
admet-249	50	34	mm	mm	NOUN
admet-249	50	35	prodigy	prodigy	NOUN
admet-249	50	36	cryoprobe	cryoprobe	NOUN
admet-249	50	37	and	and	CCONJ
admet-249	50	38	z	z	NOUN
admet-249	50	39	-	-	PUNCT
admet-249	50	40	gradient	gradient	ADJ
admet-249	50	41	accessories	accessory	NOUN
admet-249	50	42	.	.	PUNCT
admet-249	51	1	after	after	SCONJ
admet-249	51	2	lc	lc	PROPN
admet-249	51	3	separation	separation	NOUN
admet-249	51	4	and	and	CCONJ
admet-249	51	5	peak	peak	NOUN
admet-249	51	6	trapping	trap	VERB
admet-249	51	7	on	on	ADP
admet-249	51	8	the	the	DET
admet-249	51	9	spe	spe	PROPN
admet-249	51	10	unit	unit	NOUN
admet-249	51	11	,	,	PUNCT
admet-249	51	12	the	the	DET
admet-249	51	13	separated	separate	VERB
admet-249	51	14	components	component	NOUN
admet-249	51	15	were	be	AUX
admet-249	51	16	dissolved	dissolve	VERB
admet-249	51	17	in	in	ADP
admet-249	51	18	acetonitrile	acetonitrile	NOUN
admet-249	51	19	-	-	PUNCT
admet-249	51	20	d3	d3	PROPN
admet-249	51	21	and	and	CCONJ
admet-249	51	22	measured	measure	VERB
admet-249	51	23	in	in	ADP
admet-249	51	24	3	3	NUM
admet-249	51	25	mm	mm	PROPN
admet-249	51	26	tubes	tube	NOUN
admet-249	51	27	with	with	ADP
admet-249	51	28	match	match	NOUN
admet-249	51	29	inserts	insert	NOUN
admet-249	51	30	for	for	ADP
admet-249	51	31	adapting	adapt	VERB
admet-249	51	32	the	the	DET
admet-249	51	33	tubes	tube	NOUN
admet-249	51	34	to	to	ADP
admet-249	51	35	5	5	NUM
admet-249	51	36	mm	mm	PROPN
admet-249	51	37	bruker	bruker	NOUN
admet-249	51	38	spinners	spinner	NOUN
admet-249	51	39	.	.	PUNCT
admet-249	52	1	all	all	DET
admet-249	52	2	experiments	experiment	NOUN
admet-249	52	3	were	be	AUX
admet-249	52	4	carried	carry	VERB
admet-249	52	5	out	out	ADP
admet-249	52	6	at	at	ADP
admet-249	52	7	298	298	NUM
admet-249	52	8	k	k	NOUN
admet-249	52	9	using	use	VERB
admet-249	52	10	tms	tms	PROPN
admet-249	52	11	as	as	ADP
admet-249	52	12	an	an	DET
admet-249	52	13	internal	internal	ADJ
admet-249	52	14	standard	standard	NOUN
admet-249	52	15	.	.	PUNCT
admet-249	53	1	proton	proton	PROPN
admet-249	53	2	spectra	spectra	NOUN
admet-249	53	3	with	with	ADP
admet-249	53	4	spectral	spectral	ADJ
admet-249	53	5	width	width	NOUN
admet-249	53	6	of	of	ADP
admet-249	53	7	6002	6002	NUM
admet-249	53	8	hz	hz	VERB
admet-249	53	9	and	and	CCONJ
admet-249	53	10	a	a	DET
admet-249	53	11	digital	digital	ADJ
admet-249	53	12	resolution	resolution	NOUN
admet-249	53	13	of	of	ADP
admet-249	53	14	0.36	0.36	NUM
admet-249	53	15	hz	hz	VERB
admet-249	53	16	per	per	ADP
admet-249	53	17	point	point	NOUN
admet-249	53	18	were	be	AUX
admet-249	53	19	measured	measure	VERB
admet-249	53	20	with	with	ADP
admet-249	53	21	64	64	NUM
admet-249	53	22	and	and	CCONJ
admet-249	53	23	128	128	NUM
admet-249	53	24	scans	scan	NOUN
admet-249	53	25	.	.	PUNCT
admet-249	54	1	in	in	ADP
admet-249	54	2	the	the	DET
admet-249	54	3	gcosy	gcosy	NOUN
admet-249	54	4	experiment	experiment	NOUN
admet-249	54	5	,	,	PUNCT
admet-249	54	6	2048	2048	NUM
admet-249	54	7	points	point	NOUN
admet-249	54	8	in	in	ADP
admet-249	54	9	the	the	DET
admet-249	54	10	f2	f2	ADJ
admet-249	54	11	dimension	dimension	NOUN
admet-249	54	12	and	and	CCONJ
admet-249	54	13	128	128	NUM
admet-249	54	14	increments	increment	NOUN
admet-249	54	15	in	in	ADP
admet-249	54	16	the	the	DET
admet-249	54	17	f1	f1	NOUN
admet-249	54	18	dimension	dimension	NOUN
admet-249	54	19	were	be	AUX
admet-249	54	20	used	use	VERB
admet-249	54	21	.	.	PUNCT
admet-249	55	1	for	for	ADP
admet-249	55	2	each	each	DET
admet-249	55	3	increment	increment	NOUN
admet-249	55	4	,	,	PUNCT
admet-249	55	5	16	16	NUM
admet-249	55	6	scans	scan	NOUN
admet-249	55	7	and	and	CCONJ
admet-249	55	8	the	the	DET
admet-249	55	9	spectral	spectral	ADJ
admet-249	55	10	width	width	NOUN
admet-249	55	11	of	of	ADP
admet-249	55	12	6010	6010	NUM
admet-249	55	13	hz	hz	VERB
admet-249	55	14	were	be	AUX
admet-249	55	15	applied	apply	VERB
admet-249	55	16	.	.	PUNCT
admet-249	56	1	digital	digital	ADJ
admet-249	56	2	resolution	resolution	NOUN
admet-249	56	3	was	be	AUX
admet-249	56	4	5.87	5.87	NUM
admet-249	56	5	and	and	CCONJ
admet-249	56	6	93.78	93.78	NUM
admet-249	56	7	hz	hz	VERB
admet-249	56	8	per	per	ADP
admet-249	56	9	point	point	NOUN
admet-249	56	10	in	in	ADP
admet-249	56	11	f2	f2	PROPN
admet-249	56	12	and	and	CCONJ
admet-249	56	13	f1	f1	NOUN
admet-249	56	14	dimensions	dimension	NOUN
admet-249	56	15	,	,	PUNCT
admet-249	56	16	respectively	respectively	ADV
admet-249	56	17	.	.	PUNCT
admet-249	57	1	the	the	DET
admet-249	57	2	ghsqc	ghsqc	NOUN
admet-249	57	3	and	and	CCONJ
admet-249	57	4	ghmbc	ghmbc	NOUN
admet-249	57	5	spectra	spectra	NOUN
admet-249	57	6	were	be	AUX
admet-249	57	7	acquired	acquire	VERB
admet-249	57	8	with	with	ADP
admet-249	57	9	64	64	NUM
admet-249	57	10	and	and	CCONJ
admet-249	57	11	128	128	NUM
admet-249	57	12	scans	scan	NOUN
admet-249	57	13	,	,	PUNCT
admet-249	57	14	respectively	respectively	ADV
admet-249	57	15	.	.	PUNCT
admet-249	58	1	spectral	spectral	ADJ
admet-249	58	2	width	width	NOUN
admet-249	58	3	was	be	AUX
admet-249	58	4	6009	6009	NUM
admet-249	58	5	hz	hz	VERB
admet-249	58	6	in	in	ADP
admet-249	58	7	f2	f2	PROPN
admet-249	58	8	and	and	CCONJ
admet-249	58	9	20124	20124	NUM
admet-249	58	10	hz	hz	VERB
admet-249	58	11	in	in	ADP
admet-249	58	12	f1	f1	NOUN
admet-249	58	13	dimension	dimension	NOUN
admet-249	58	14	for	for	ADP
admet-249	58	15	both	both	DET
admet-249	58	16	experiments	experiment	NOUN
admet-249	58	17	.	.	PUNCT
admet-249	59	1	1k	1k	NUM
admet-249	59	2	data	datum	NOUN
admet-249	59	3	points	point	NOUN
admet-249	59	4	were	be	AUX
admet-249	59	5	applied	apply	VERB
admet-249	59	6	in	in	ADP
admet-249	59	7	the	the	DET
admet-249	59	8	time	time	NOUN
admet-249	59	9	domains	domain	NOUN
admet-249	59	10	and	and	CCONJ
admet-249	59	11	for	for	SCONJ
admet-249	59	12	each	each	DET
admet-249	59	13	data	datum	NOUN
admet-249	59	14	set	set	VERB
admet-249	59	15	256	256	NUM
admet-249	59	16	increments	increment	NOUN
admet-249	59	17	were	be	AUX
admet-249	59	18	collected	collect	VERB
admet-249	59	19	.	.	PUNCT
admet-249	60	1	the	the	DET
admet-249	60	2	resulting	result	VERB
admet-249	60	3	digital	digital	ADJ
admet-249	60	4	resolution	resolution	NOUN
admet-249	60	5	was	be	AUX
admet-249	60	6	5.86	5.86	NUM
admet-249	60	7	hz	hz	NOUN
admet-249	60	8	per	per	ADP
admet-249	60	9	point	point	NOUN
admet-249	60	10	in	in	ADP
admet-249	60	11	f2	f2	ADJ
admet-249	60	12	dimension	dimension	NOUN
admet-249	60	13	and	and	CCONJ
admet-249	60	14	314.4	314.4	NUM
admet-249	60	15	hz	hz	NOUN
admet-249	60	16	per	per	ADP
admet-249	60	17	point	point	NOUN
admet-249	60	18	in	in	ADP
admet-249	60	19	f1	f1	ADJ
admet-249	60	20	dimension	dimension	NOUN
admet-249	60	21	.	.	PUNCT
admet-249	61	1	results	result	NOUN
admet-249	61	2	and	and	CCONJ
admet-249	61	3	discussion	discussion	VERB
admet-249	61	4	the	the	DET
admet-249	61	5	condensation	condensation	NOUN
admet-249	61	6	reaction	reaction	NOUN
admet-249	61	7	of	of	ADP
admet-249	61	8	carbohydrazide	carbohydrazide	NOUN
admet-249	61	9	and	and	CCONJ
admet-249	61	10	salicylaldehyde	salicylaldehyde	NOUN
admet-249	61	11	was	be	AUX
admet-249	61	12	performed	perform	VERB
admet-249	61	13	in	in	ADP
admet-249	61	14	methanol	methanol	NOUN
admet-249	61	15	and	and	CCONJ
admet-249	61	16	the	the	DET
admet-249	61	17	reaction	reaction	NOUN
admet-249	61	18	products	product	NOUN
admet-249	61	19	were	be	AUX
admet-249	61	20	subsequently	subsequently	ADV
admet-249	61	21	analysed	analyse	VERB
admet-249	61	22	by	by	ADP
admet-249	61	23	lc	lc	PROPN
admet-249	61	24	-	-	PUNCT
admet-249	61	25	dad	dad	NOUN
admet-249	61	26	-	-	PUNCT
admet-249	61	27	spe	spe	PROPN
admet-249	61	28	-	-	PUNCT
admet-249	61	29	nmr	nmr	NOUN
admet-249	61	30	method	method	NOUN
admet-249	61	31	.	.	PUNCT
admet-249	62	1	prior	prior	ADV
admet-249	62	2	to	to	ADP
admet-249	62	3	lc	lc	PROPN
admet-249	62	4	-	-	PUNCT
admet-249	62	5	dad	dad	NOUN
admet-249	62	6	-	-	PUNCT
admet-249	62	7	spe	spe	PROPN
admet-249	62	8	-	-	PUNCT
admet-249	62	9	nmr	nmr	NOUN
admet-249	62	10	analysis	analysis	NOUN
admet-249	62	11	,	,	PUNCT
admet-249	62	12	a	a	DET
admet-249	62	13	chromatographic	chromatographic	ADJ
admet-249	62	14	method	method	NOUN
admet-249	62	15	was	be	AUX
admet-249	62	16	developed	develop	VERB
admet-249	62	17	and	and	CCONJ
admet-249	62	18	optimised	optimise	VERB
admet-249	62	19	.	.	PUNCT
admet-249	63	1	chromatographic	chromatographic	ADJ
admet-249	63	2	separation	separation	NOUN
admet-249	63	3	of	of	ADP
admet-249	63	4	the	the	DET
admet-249	63	5	individual	individual	ADJ
admet-249	63	6	products	product	NOUN
admet-249	63	7	and	and	CCONJ
admet-249	63	8	reactants	reactant	NOUN
admet-249	63	9	was	be	AUX
admet-249	63	10	readily	readily	ADV
admet-249	63	11	achieved	achieve	VERB
admet-249	63	12	by	by	ADP
admet-249	63	13	using	use	VERB
admet-249	63	14	an	an	DET
admet-249	63	15	isocratic	isocratic	ADJ
admet-249	63	16	acetonitrile	acetonitrile	ADJ
admet-249	63	17	-	-	PUNCT
admet-249	63	18	phosphate	phosphate	NOUN
admet-249	63	19	buffer	buffer	NOUN
admet-249	63	20	admet	admet	NOUN
admet-249	63	21	&	&	CCONJ
admet-249	63	22	dmpk	dmpk	PROPN
admet-249	63	23	3(4	3(4	NUM
admet-249	63	24	)	)	PUNCT
admet-249	63	25	(	(	PUNCT
admet-249	63	26	2015	2015	NUM
admet-249	63	27	)	)	PUNCT
admet-249	63	28	352	352	NUM
admet-249	63	29	-	-	SYM
admet-249	63	30	358	358	NUM
admet-249	63	31	carbohydrazide	carbohydrazide	ADJ
admet-249	63	32	reaction	reaction	NOUN
admet-249	63	33	monitoring	monitoring	NOUN
admet-249	63	34	by	by	ADP
admet-249	63	35	lc	lc	PROPN
admet-249	63	36	-	-	PUNCT
admet-249	63	37	dad	dad	NOUN
admet-249	63	38	-	-	PUNCT
admet-249	63	39	spe	spe	PROPN
admet-249	63	40	-	-	PUNCT
admet-249	63	41	nmr	nmr	NOUN
admet-249	63	42	doi	doi	NOUN
admet-249	63	43	:	:	PUNCT
admet-249	63	44	10.5599	10.5599	NUM
admet-249	63	45	/	/	SYM
admet-249	63	46	admet.3.4.249	admet.3.4.249	NOUN
admet-249	63	47	355	355	NUM
admet-249	63	48	mobile	mobile	ADJ
admet-249	63	49	phase	phase	NOUN
admet-249	63	50	.	.	PUNCT
admet-249	64	1	to	to	PART
admet-249	64	2	identify	identify	VERB
admet-249	64	3	and	and	CCONJ
admet-249	64	4	structurally	structurally	ADV
admet-249	64	5	characterise	characterise	VERB
admet-249	64	6	reaction	reaction	NOUN
admet-249	64	7	components	component	NOUN
admet-249	64	8	,	,	PUNCT
admet-249	64	9	we	we	PRON
admet-249	64	10	performed	perform	VERB
admet-249	64	11	lc	lc	PROPN
admet-249	64	12	-	-	PUNCT
admet-249	64	13	dad	dad	NOUN
admet-249	64	14	-	-	ADJ
admet-249	64	15	spenmr	spenmr	ADJ
admet-249	64	16	analysis	analysis	NOUN
admet-249	64	17	.	.	PUNCT
admet-249	65	1	two	two	NUM
admet-249	65	2	different	different	ADJ
admet-249	65	3	approaches	approach	NOUN
admet-249	65	4	were	be	AUX
admet-249	65	5	used	use	VERB
admet-249	65	6	.	.	PUNCT
admet-249	66	1	in	in	ADP
admet-249	66	2	the	the	DET
admet-249	66	3	first	first	ADJ
admet-249	66	4	one	one	NUM
admet-249	66	5	,	,	PUNCT
admet-249	66	6	we	we	PRON
admet-249	66	7	filtered	filter	VERB
admet-249	66	8	the	the	DET
admet-249	66	9	reaction	reaction	NOUN
admet-249	66	10	mixture	mixture	NOUN
admet-249	66	11	and	and	CCONJ
admet-249	66	12	dissolved	dissolve	VERB
admet-249	66	13	the	the	DET
admet-249	66	14	crude	crude	ADJ
admet-249	66	15	products	product	NOUN
admet-249	66	16	iii	iii	NOUN
admet-249	66	17	and	and	CCONJ
admet-249	66	18	iv	iv	NOUN
admet-249	66	19	together	together	ADV
admet-249	66	20	with	with	ADP
admet-249	66	21	reactants	reactant	NOUN
admet-249	66	22	in	in	ADP
admet-249	66	23	acetonitrile	acetonitrile	NOUN
admet-249	66	24	and	and	CCONJ
admet-249	66	25	injected	inject	VERB
admet-249	66	26	25	25	NUM
admet-249	66	27	µl	µl	NOUN
admet-249	66	28	of	of	ADP
admet-249	66	29	the	the	DET
admet-249	66	30	solution	solution	NOUN
admet-249	66	31	into	into	ADP
admet-249	66	32	the	the	DET
admet-249	66	33	lc	lc	NOUN
admet-249	66	34	-	-	PUNCT
admet-249	66	35	spe	spe	NOUN
admet-249	66	36	system	system	NOUN
admet-249	66	37	.	.	PUNCT
admet-249	67	1	the	the	DET
admet-249	67	2	lc	lc	PROPN
admet-249	67	3	-	-	PUNCT
admet-249	67	4	dad	dad	NOUN
admet-249	67	5	chromatogram	chromatogram	NOUN
admet-249	67	6	of	of	ADP
admet-249	67	7	this	this	DET
admet-249	67	8	standard	standard	ADJ
admet-249	67	9	mixture	mixture	NOUN
admet-249	67	10	is	be	AUX
admet-249	67	11	presented	present	VERB
admet-249	67	12	in	in	ADP
admet-249	67	13	figure	figure	NOUN
admet-249	67	14	2a	2a	NUM
admet-249	67	15	.	.	PUNCT
admet-249	68	1	in	in	ADP
admet-249	68	2	the	the	DET
admet-249	68	3	second	second	ADJ
admet-249	68	4	approach	approach	NOUN
admet-249	68	5	,	,	PUNCT
admet-249	68	6	we	we	PRON
admet-249	68	7	took	take	VERB
admet-249	68	8	aliquots	aliquot	NOUN
admet-249	68	9	directly	directly	ADV
admet-249	68	10	from	from	ADP
admet-249	68	11	the	the	DET
admet-249	68	12	reaction	reaction	NOUN
admet-249	68	13	mixture	mixture	NOUN
admet-249	68	14	(	(	PUNCT
admet-249	68	15	20	20	NUM
admet-249	68	16	µl	µl	NOUN
admet-249	68	17	)	)	PUNCT
admet-249	68	18	,	,	PUNCT
admet-249	68	19	added	add	VERB
admet-249	68	20	480	480	NUM
admet-249	68	21	μl	μl	NUM
admet-249	68	22	of	of	ADP
admet-249	68	23	acetonitrile	acetonitrile	NOUN
admet-249	68	24	and	and	CCONJ
admet-249	68	25	then	then	ADV
admet-249	68	26	performed	perform	VERB
admet-249	68	27	the	the	DET
admet-249	68	28	analysis	analysis	NOUN
admet-249	68	29	by	by	ADP
admet-249	68	30	injecting	inject	VERB
admet-249	68	31	25	25	NUM
admet-249	68	32	µl	µl	NOUN
admet-249	68	33	of	of	ADP
admet-249	68	34	the	the	DET
admet-249	68	35	solution	solution	NOUN
admet-249	68	36	.	.	PUNCT
admet-249	69	1	the	the	DET
admet-249	69	2	chromatogram	chromatogram	NOUN
admet-249	69	3	is	be	AUX
admet-249	69	4	shown	show	VERB
admet-249	69	5	in	in	ADP
admet-249	69	6	figure	figure	NOUN
admet-249	69	7	2b	2b	NOUN
admet-249	69	8	.	.	PUNCT
admet-249	70	1	figure	figure	NOUN
admet-249	70	2	2	2	NUM
admet-249	70	3	.	.	PUNCT
admet-249	70	4	lc	lc	NOUN
admet-249	70	5	-	-	PUNCT
admet-249	70	6	dad	dad	NOUN
admet-249	70	7	chromatogram	chromatogram	PROPN
admet-249	70	8	of	of	ADP
admet-249	70	9	(	(	PUNCT
admet-249	70	10	a	a	X
admet-249	70	11	)	)	PUNCT
admet-249	70	12	the	the	DET
admet-249	70	13	standard	standard	ADJ
admet-249	70	14	reaction	reaction	NOUN
admet-249	70	15	mixture	mixture	NOUN
admet-249	70	16	,	,	PUNCT
admet-249	70	17	(	(	PUNCT
admet-249	70	18	b	b	X
admet-249	70	19	)	)	PUNCT
admet-249	70	20	the	the	DET
admet-249	70	21	reaction	reaction	NOUN
admet-249	70	22	mixture	mixture	NOUN
admet-249	70	23	aliquot	aliquot	NOUN
admet-249	70	24	collected	collect	VERB
admet-249	70	25	5	5	NUM
admet-249	70	26	min	min	NOUN
admet-249	70	27	after	after	SCONJ
admet-249	70	28	the	the	DET
admet-249	70	29	reaction	reaction	NOUN
admet-249	70	30	start	start	VERB
admet-249	70	31	.	.	PUNCT
admet-249	71	1	the	the	DET
admet-249	71	2	peaks	peak	NOUN
admet-249	71	3	designated	designate	VERB
admet-249	71	4	with	with	ADP
admet-249	71	5	asterisks	asterisk	NOUN
admet-249	71	6	are	be	AUX
admet-249	71	7	unknown	unknown	ADJ
admet-249	71	8	compounds	compound	NOUN
admet-249	71	9	.	.	PUNCT
admet-249	72	1	aliquots	aliquot	NOUN
admet-249	72	2	were	be	AUX
admet-249	72	3	collected	collect	VERB
admet-249	72	4	at	at	ADP
admet-249	72	5	the	the	DET
admet-249	72	6	beginning	beginning	NOUN
admet-249	72	7	of	of	ADP
admet-249	72	8	the	the	DET
admet-249	72	9	reaction	reaction	NOUN
admet-249	72	10	and	and	CCONJ
admet-249	72	11	after	after	ADP
admet-249	72	12	3	3	NUM
admet-249	72	13	,	,	PUNCT
admet-249	72	14	5	5	NUM
admet-249	72	15	,	,	PUNCT
admet-249	72	16	10	10	NUM
admet-249	72	17	,	,	PUNCT
admet-249	72	18	25	25	NUM
admet-249	72	19	and	and	CCONJ
admet-249	72	20	40	40	NUM
admet-249	72	21	minutes	minute	NOUN
admet-249	72	22	.	.	PUNCT
admet-249	73	1	it	it	PRON
admet-249	73	2	is	be	AUX
admet-249	73	3	seen	see	VERB
admet-249	73	4	in	in	ADP
admet-249	73	5	the	the	DET
admet-249	73	6	figure	figure	NOUN
admet-249	73	7	2	2	NUM
admet-249	73	8	that	that	SCONJ
admet-249	73	9	two	two	NUM
admet-249	73	10	products	product	NOUN
admet-249	73	11	were	be	AUX
admet-249	73	12	formed	form	VERB
admet-249	73	13	,	,	PUNCT
admet-249	73	14	iii	iii	PROPN
admet-249	73	15	and	and	CCONJ
admet-249	73	16	iv	iv	NUM
admet-249	73	17	with	with	ADP
admet-249	73	18	the	the	DET
admet-249	73	19	retention	retention	NOUN
admet-249	73	20	times	time	NOUN
admet-249	73	21	of	of	ADP
admet-249	73	22	2.6	2.6	NUM
admet-249	73	23	and	and	CCONJ
admet-249	73	24	5.9	5.9	NUM
admet-249	73	25	minutes	minute	NOUN
admet-249	73	26	,	,	PUNCT
admet-249	73	27	respectively	respectively	ADV
admet-249	73	28	.	.	PUNCT
admet-249	74	1	in	in	ADP
admet-249	74	2	chromatograms	chromatogram	NOUN
admet-249	74	3	collected	collect	VERB
admet-249	74	4	during	during	ADP
admet-249	74	5	the	the	DET
admet-249	74	6	reaction	reaction	NOUN
admet-249	74	7	course	course	NOUN
admet-249	74	8	those	those	DET
admet-249	74	9	peaks	peak	NOUN
admet-249	74	10	gradually	gradually	ADV
admet-249	74	11	increased	increase	VERB
admet-249	74	12	while	while	SCONJ
admet-249	74	13	i	i	PRON
admet-249	74	14	and	and	CCONJ
admet-249	74	15	ii	ii	PROPN
admet-249	74	16	decreased	decrease	VERB
admet-249	74	17	and	and	CCONJ
admet-249	74	18	vanished	vanish	VERB
admet-249	74	19	in	in	ADP
admet-249	74	20	the	the	DET
admet-249	74	21	interval	interval	NOUN
admet-249	74	22	between	between	ADP
admet-249	74	23	5	5	NUM
admet-249	74	24	and	and	CCONJ
admet-249	74	25	10	10	NUM
admet-249	74	26	minutes	minute	NOUN
admet-249	74	27	thus	thus	ADV
admet-249	74	28	indicating	indicate	VERB
admet-249	74	29	the	the	DET
admet-249	74	30	end	end	NOUN
admet-249	74	31	of	of	ADP
admet-249	74	32	the	the	DET
admet-249	74	33	habinovec	habinovec	PROPN
admet-249	74	34	et	et	PROPN
admet-249	74	35	al	al	PROPN
admet-249	74	36	.	.	PROPN
admet-249	74	37	admet	admet	PROPN
admet-249	74	38	&	&	CCONJ
admet-249	74	39	dmpk	dmpk	PROPN
admet-249	74	40	3(4	3(4	NUM
admet-249	74	41	)	)	PUNCT
admet-249	74	42	(	(	PUNCT
admet-249	74	43	2015	2015	NUM
admet-249	74	44	)	)	PUNCT
admet-249	74	45	352	352	NUM
admet-249	74	46	-	-	SYM
admet-249	74	47	358	358	NUM
admet-249	74	48	356	356	NUM
admet-249	74	49	reaction	reaction	NOUN
admet-249	74	50	.	.	PUNCT
admet-249	75	1	this	this	DET
admet-249	75	2	finding	finding	NOUN
admet-249	75	3	is	be	AUX
admet-249	75	4	somewhat	somewhat	ADV
admet-249	75	5	different	different	ADJ
admet-249	75	6	from	from	ADP
admet-249	75	7	that	that	PRON
admet-249	75	8	previously	previously	ADV
admet-249	75	9	observed	observe	VERB
admet-249	75	10	by	by	ADP
admet-249	75	11	in	in	ADP
admet-249	75	12	-	-	PUNCT
admet-249	75	13	line	line	NOUN
admet-249	75	14	vibrational	vibrational	ADJ
admet-249	75	15	spectroscopy	spectroscopy	NOUN
admet-249	75	16	and	and	CCONJ
admet-249	75	17	statistical	statistical	ADJ
admet-249	75	18	methods	method	NOUN
admet-249	75	19	[	[	X
admet-249	75	20	11	11	NUM
admet-249	75	21	]	]	PUNCT
admet-249	75	22	where	where	SCONJ
admet-249	75	23	the	the	DET
admet-249	75	24	reaction	reaction	NOUN
admet-249	75	25	endpoint	endpoint	VERB
admet-249	75	26	in	in	ADP
admet-249	75	27	methanol	methanol	NOUN
admet-249	75	28	was	be	AUX
admet-249	75	29	estimated	estimate	VERB
admet-249	75	30	to	to	PART
admet-249	75	31	be	be	AUX
admet-249	75	32	around	around	ADV
admet-249	75	33	30	30	NUM
admet-249	75	34	minutes	minute	NOUN
admet-249	75	35	.	.	PUNCT
admet-249	76	1	according	accord	VERB
admet-249	76	2	to	to	ADP
admet-249	76	3	lc	lc	PROPN
admet-249	76	4	area	area	PROPN
admet-249	76	5	peak	peak	NOUN
admet-249	76	6	integrals	integral	VERB
admet-249	76	7	condensation	condensation	NOUN
admet-249	76	8	reactions	reaction	NOUN
admet-249	76	9	gave	give	VERB
admet-249	76	10	48	48	NUM
admet-249	76	11	%	%	NOUN
admet-249	76	12	of	of	ADP
admet-249	76	13	iii	iii	NUM
admet-249	76	14	and	and	CCONJ
admet-249	76	15	52	52	NUM
admet-249	76	16	%	%	NOUN
admet-249	76	17	of	of	ADP
admet-249	76	18	iv	iv	NUM
admet-249	76	19	which	which	PRON
admet-249	76	20	was	be	AUX
admet-249	76	21	similar	similar	ADJ
admet-249	76	22	to	to	ADP
admet-249	76	23	previous	previous	ADJ
admet-249	76	24	results	result	NOUN
admet-249	76	25	.	.	PUNCT
admet-249	77	1	a	a	DET
admet-249	77	2	close	close	ADJ
admet-249	77	3	inspection	inspection	NOUN
admet-249	77	4	of	of	ADP
admet-249	77	5	chromatogram	chromatogram	NOUN
admet-249	77	6	depicted	depict	VERB
admet-249	77	7	in	in	ADP
admet-249	77	8	figure	figure	NOUN
admet-249	77	9	2b	2b	NOUN
admet-249	77	10	reveals	reveal	VERB
admet-249	77	11	two	two	NUM
admet-249	77	12	additional	additional	ADJ
admet-249	77	13	peaks	peak	NOUN
admet-249	77	14	with	with	ADP
admet-249	77	15	retention	retention	NOUN
admet-249	77	16	times	time	NOUN
admet-249	77	17	around	around	ADP
admet-249	77	18	4	4	NUM
admet-249	77	19	minutes	minute	NOUN
admet-249	77	20	.	.	PUNCT
admet-249	78	1	unfortunately	unfortunately	ADV
admet-249	78	2	,	,	PUNCT
admet-249	78	3	those	those	PRON
admet-249	78	4	could	could	AUX
admet-249	78	5	n’t	not	PART
admet-249	78	6	be	be	AUX
admet-249	78	7	trapped	trap	VERB
admet-249	78	8	on	on	ADP
admet-249	78	9	the	the	DET
admet-249	78	10	cartridges	cartridge	NOUN
admet-249	78	11	used	use	VERB
admet-249	78	12	in	in	ADP
admet-249	78	13	this	this	DET
admet-249	78	14	study	study	NOUN
admet-249	78	15	and	and	CCONJ
admet-249	78	16	further	further	ADJ
admet-249	78	17	method	method	NOUN
admet-249	78	18	development	development	NOUN
admet-249	78	19	is	be	AUX
admet-249	78	20	needed	need	VERB
admet-249	78	21	to	to	PART
admet-249	78	22	resolve	resolve	VERB
admet-249	78	23	their	their	PRON
admet-249	78	24	identity	identity	NOUN
admet-249	78	25	and	and	CCONJ
admet-249	78	26	structure	structure	NOUN
admet-249	78	27	.	.	PUNCT
admet-249	79	1	to	to	PART
admet-249	79	2	identify	identify	VERB
admet-249	79	3	and	and	CCONJ
admet-249	79	4	structurally	structurally	ADV
admet-249	79	5	characterise	characterise	VERB
admet-249	79	6	the	the	DET
admet-249	79	7	reaction	reaction	NOUN
admet-249	79	8	products	product	NOUN
admet-249	79	9	iii	iii	PROPN
admet-249	79	10	and	and	CCONJ
admet-249	79	11	iv	iv	NUM
admet-249	79	12	,	,	PUNCT
admet-249	79	13	the	the	DET
admet-249	79	14	contents	content	NOUN
admet-249	79	15	of	of	ADP
admet-249	79	16	their	their	PRON
admet-249	79	17	lc	lc	NOUN
admet-249	79	18	peaks	peak	NOUN
admet-249	79	19	were	be	AUX
admet-249	79	20	sent	send	VERB
admet-249	79	21	to	to	PART
admet-249	79	22	post	post	VERB
admet-249	79	23	column	column	NOUN
admet-249	79	24	spe	spe	NOUN
admet-249	79	25	trapping	trap	VERB
admet-249	79	26	for	for	ADP
admet-249	79	27	pre	pre	ADJ
admet-249	79	28	-	-	NOUN
admet-249	79	29	concentration	concentration	NOUN
admet-249	79	30	prior	prior	ADV
admet-249	79	31	to	to	ADP
admet-249	79	32	nmr	nmr	NOUN
admet-249	79	33	analysis	analysis	NOUN
admet-249	79	34	in	in	ADP
admet-249	79	35	order	order	NOUN
admet-249	79	36	to	to	PART
admet-249	79	37	achieve	achieve	VERB
admet-249	79	38	a	a	DET
admet-249	79	39	better	well	ADJ
admet-249	79	40	signal	signal	NOUN
admet-249	79	41	-	-	PUNCT
admet-249	79	42	to	to	ADP
admet-249	79	43	-	-	PUNCT
admet-249	79	44	noise	noise	NOUN
admet-249	79	45	ratio	ratio	NOUN
admet-249	79	46	.	.	PUNCT
admet-249	80	1	subsequently	subsequently	ADV
admet-249	80	2	,	,	PUNCT
admet-249	80	3	the	the	DET
admet-249	80	4	spe	spe	ADJ
admet-249	80	5	cartridges	cartridge	NOUN
admet-249	80	6	were	be	AUX
admet-249	80	7	dried	dry	VERB
admet-249	80	8	with	with	ADP
admet-249	80	9	nitrogen	nitrogen	NOUN
admet-249	80	10	gas	gas	NOUN
admet-249	80	11	before	before	ADP
admet-249	80	12	peak	peak	NOUN
admet-249	80	13	elution	elution	NOUN
admet-249	80	14	.	.	PUNCT
admet-249	81	1	deuterated	deuterate	VERB
admet-249	81	2	acetonitrile	acetonitrile	NOUN
admet-249	81	3	was	be	AUX
admet-249	81	4	used	use	VERB
admet-249	81	5	to	to	PART
admet-249	81	6	elute	elute	VERB
admet-249	81	7	and	and	CCONJ
admet-249	81	8	transfer	transfer	VERB
admet-249	81	9	the	the	DET
admet-249	81	10	peaks	peak	NOUN
admet-249	81	11	from	from	ADP
admet-249	81	12	the	the	DET
admet-249	81	13	cartridges	cartridge	NOUN
admet-249	81	14	to	to	ADP
admet-249	81	15	3	3	NUM
admet-249	81	16	mm	mm	PROPN
admet-249	81	17	nmr	nmr	NOUN
admet-249	81	18	tubes	tube	NOUN
admet-249	81	19	.	.	PUNCT
admet-249	82	1	to	to	PART
admet-249	82	2	record	record	VERB
admet-249	82	3	one	one	NUM
admet-249	82	4	-	-	PUNCT
admet-249	82	5	dimensional	dimensional	ADJ
admet-249	82	6	proton	proton	NOUN
admet-249	82	7	and	and	CCONJ
admet-249	82	8	two	two	NUM
admet-249	82	9	-	-	PUNCT
admet-249	82	10	dimensional	dimensional	ADJ
admet-249	82	11	cosy	cosy	ADJ
admet-249	82	12	spectra	spectra	NOUN
admet-249	82	13	,	,	PUNCT
admet-249	82	14	a	a	DET
admet-249	82	15	single	single	ADJ
admet-249	82	16	trapping	trapping	NOUN
admet-249	82	17	was	be	AUX
admet-249	82	18	sufficient	sufficient	ADJ
admet-249	82	19	for	for	ADP
admet-249	82	20	the	the	DET
admet-249	82	21	compound	compound	NOUN
admet-249	82	22	iv	iv	X
admet-249	82	23	(	(	PUNCT
admet-249	82	24	figures	figure	NOUN
admet-249	82	25	3	3	NUM
admet-249	82	26	and	and	CCONJ
admet-249	82	27	4	4	NUM
admet-249	82	28	)	)	PUNCT
admet-249	82	29	,	,	PUNCT
admet-249	82	30	while	while	SCONJ
admet-249	82	31	multiple	multiple	ADJ
admet-249	82	32	trapping	trap	VERB
admet-249	82	33	option	option	NOUN
admet-249	82	34	was	be	AUX
admet-249	82	35	used	use	VERB
admet-249	82	36	to	to	PART
admet-249	82	37	record	record	VERB
admet-249	82	38	heteronuclear	heteronuclear	NOUN
admet-249	82	39	two	two	NUM
admet-249	82	40	-	-	PUNCT
admet-249	82	41	dimensional	dimensional	ADJ
admet-249	82	42	spectra	spectra	NOUN
admet-249	82	43	(	(	PUNCT
admet-249	82	44	hsqc	hsqc	NOUN
admet-249	82	45	and	and	CCONJ
admet-249	82	46	hmbc	hmbc	PROPN
admet-249	82	47	)	)	PUNCT
admet-249	82	48	.	.	PUNCT
admet-249	83	1	figure	figure	VERB
admet-249	83	2	3	3	NUM
admet-249	83	3	.	.	PUNCT
admet-249	84	1	an	an	DET
admet-249	84	2	expanded	expand	VERB
admet-249	84	3	region	region	NOUN
admet-249	84	4	of	of	ADP
admet-249	84	5	1	1	NUM
admet-249	84	6	h	h	NOUN
admet-249	84	7	nmr	nmr	NOUN
admet-249	84	8	spectrum	spectrum	NOUN
admet-249	84	9	of	of	ADP
admet-249	84	10	iv	iv	NUM
admet-249	84	11	obtained	obtain	VERB
admet-249	84	12	in	in	ADP
admet-249	84	13	lc	lc	PROPN
admet-249	84	14	-	-	PUNCT
admet-249	84	15	spe	spe	NOUN
admet-249	84	16	-	-	PUNCT
admet-249	84	17	nmr	nmr	NOUN
admet-249	84	18	mode	mode	NOUN
admet-249	84	19	for	for	ADP
admet-249	84	20	:	:	PUNCT
admet-249	84	21	(	(	PUNCT
admet-249	84	22	a	a	X
admet-249	84	23	)	)	PUNCT
admet-249	84	24	standard	standard	ADJ
admet-249	84	25	reaction	reaction	NOUN
admet-249	84	26	mixture	mixture	NOUN
admet-249	84	27	(	(	PUNCT
admet-249	84	28	initial	initial	ADJ
admet-249	84	29	mass	mass	NOUN
admet-249	84	30	1.95	1.95	NUM
admet-249	84	31	μg	μg	NOUN
admet-249	84	32	,	,	PUNCT
admet-249	84	33	64	64	NUM
admet-249	84	34	scans	scan	NOUN
admet-249	84	35	,	,	PUNCT
admet-249	84	36	6	6	NUM
admet-249	84	37	min	min	NOUN
admet-249	84	38	)	)	PUNCT
admet-249	84	39	(	(	PUNCT
admet-249	84	40	b	b	X
admet-249	84	41	)	)	PUNCT
admet-249	84	42	reaction	reaction	NOUN
admet-249	84	43	mixture	mixture	NOUN
admet-249	84	44	aliquot	aliquot	NOUN
admet-249	84	45	collected	collect	VERB
admet-249	84	46	after	after	ADP
admet-249	84	47	5	5	NUM
admet-249	84	48	min	min	NOUN
admet-249	84	49	(	(	PUNCT
admet-249	84	50	64	64	NUM
admet-249	84	51	scans	scan	NOUN
admet-249	84	52	,	,	PUNCT
admet-249	84	53	6	6	NUM
admet-249	84	54	min	min	NOUN
admet-249	84	55	)	)	PUNCT
admet-249	84	56	and	and	CCONJ
admet-249	84	57	(	(	PUNCT
admet-249	84	58	c	c	X
admet-249	84	59	)	)	PUNCT
admet-249	84	60	(	(	PUNCT
admet-249	84	61	128	128	NUM
admet-249	84	62	scans	scan	NOUN
admet-249	84	63	,	,	PUNCT
admet-249	84	64	12	12	NUM
admet-249	84	65	min	min	NOUN
admet-249	84	66	)	)	PUNCT
admet-249	84	67	.	.	PUNCT
admet-249	85	1	it	it	PRON
admet-249	85	2	is	be	AUX
admet-249	85	3	noteworthy	noteworthy	ADJ
admet-249	85	4	to	to	PART
admet-249	85	5	say	say	VERB
admet-249	85	6	that	that	SCONJ
admet-249	85	7	the	the	DET
admet-249	85	8	initial	initial	ADJ
admet-249	85	9	amount	amount	NOUN
admet-249	85	10	of	of	ADP
admet-249	85	11	the	the	DET
admet-249	85	12	compound	compound	NOUN
admet-249	85	13	iv	iv	PART
admet-249	85	14	to	to	PART
admet-249	85	15	record	record	VERB
admet-249	85	16	the	the	DET
admet-249	85	17	proton	proton	NOUN
admet-249	85	18	spectrum	spectrum	NOUN
admet-249	85	19	displayed	display	VERB
admet-249	85	20	in	in	ADP
admet-249	85	21	figure	figure	NOUN
admet-249	85	22	3a	3a	NUM
admet-249	85	23	was	be	AUX
admet-249	85	24	only	only	ADV
admet-249	85	25	1.95	1.95	NUM
admet-249	85	26	μg	μg	NOUN
admet-249	85	27	.	.	PUNCT
admet-249	86	1	the	the	DET
admet-249	86	2	concentration	concentration	NOUN
admet-249	86	3	of	of	ADP
admet-249	86	4	iv	iv	NUM
admet-249	86	5	was	be	AUX
admet-249	86	6	even	even	ADV
admet-249	86	7	lower	low	ADJ
admet-249	86	8	in	in	ADP
admet-249	86	9	the	the	DET
admet-249	86	10	samples	sample	NOUN
admet-249	86	11	collected	collect	VERB
admet-249	86	12	directly	directly	ADV
admet-249	86	13	from	from	ADP
admet-249	86	14	the	the	DET
admet-249	86	15	reaction	reaction	NOUN
admet-249	86	16	mixture	mixture	NOUN
admet-249	86	17	and	and	CCONJ
admet-249	86	18	satisfactory	satisfactory	ADJ
admet-249	86	19	proton	proton	NOUN
admet-249	86	20	spectrum	spectrum	NOUN
admet-249	86	21	was	be	AUX
admet-249	86	22	obtained	obtain	VERB
admet-249	86	23	with	with	ADP
admet-249	86	24	128	128	NUM
admet-249	86	25	scans	scan	NOUN
admet-249	86	26	(	(	PUNCT
admet-249	86	27	figure	figure	NOUN
admet-249	86	28	3c	3c	NUM
admet-249	86	29	)	)	PUNCT
admet-249	86	30	.	.	PUNCT
admet-249	87	1	furthermore	furthermore	ADV
admet-249	87	2	,	,	PUNCT
admet-249	87	3	very	very	ADV
admet-249	87	4	good	good	ADJ
admet-249	87	5	signal	signal	NOUN
admet-249	87	6	-	-	PUNCT
admet-249	87	7	to	to	ADP
admet-249	87	8	-	-	PUNCT
admet-249	87	9	noise	noise	NOUN
admet-249	87	10	ratio	ratio	NOUN
admet-249	87	11	was	be	AUX
admet-249	87	12	observed	observe	VERB
admet-249	87	13	also	also	ADV
admet-249	87	14	in	in	ADP
admet-249	87	15	the	the	DET
admet-249	87	16	cosy	cosy	NOUN
admet-249	87	17	spectrum	spectrum	NOUN
admet-249	87	18	of	of	ADP
admet-249	87	19	iv	iv	NUM
admet-249	87	20	depicted	depict	VERB
admet-249	87	21	in	in	ADP
admet-249	87	22	figure	figure	NOUN
admet-249	87	23	4	4	NUM
admet-249	87	24	with	with	ADP
admet-249	87	25	the	the	DET
admet-249	87	26	initial	initial	ADJ
admet-249	87	27	amount	amount	NOUN
admet-249	87	28	of	of	ADP
admet-249	87	29	only	only	ADV
admet-249	87	30	24	24	NUM
admet-249	87	31	μg	μg	NOUN
admet-249	87	32	.	.	PUNCT
admet-249	88	1	this	this	PRON
admet-249	88	2	clearly	clearly	ADV
admet-249	88	3	demonstrates	demonstrate	VERB
admet-249	88	4	the	the	DET
admet-249	88	5	advantage	advantage	NOUN
admet-249	88	6	of	of	ADP
admet-249	88	7	using	use	VERB
admet-249	88	8	lc	lc	NOUN
admet-249	88	9	-	-	PUNCT
admet-249	88	10	spenmr	spenmr	ADJ
admet-249	88	11	setup	setup	NOUN
admet-249	88	12	with	with	ADP
admet-249	88	13	prodigy	prodigy	NOUN
admet-249	88	14	cryoprobe	cryoprobe	NOUN
admet-249	88	15	for	for	ADP
admet-249	88	16	detection	detection	NOUN
admet-249	88	17	and	and	CCONJ
admet-249	88	18	identification	identification	NOUN
admet-249	88	19	of	of	ADP
admet-249	88	20	low	low	ADJ
admet-249	88	21	concentrated	concentrated	ADJ
admet-249	88	22	samples	sample	NOUN
admet-249	88	23	.	.	PUNCT
admet-249	89	1	the	the	DET
admet-249	89	2	structure	structure	NOUN
admet-249	89	3	of	of	ADP
admet-249	89	4	the	the	DET
admet-249	89	5	compounds	compound	NOUN
admet-249	89	6	was	be	AUX
admet-249	89	7	unambiguously	unambiguously	ADV
admet-249	89	8	confirmed	confirm	VERB
admet-249	89	9	by	by	ADP
admet-249	89	10	the	the	DET
admet-249	89	11	analysis	analysis	NOUN
admet-249	89	12	of	of	ADP
admet-249	89	13	the	the	DET
admet-249	89	14	recorded	record	VERB
admet-249	89	15	one(1h	one(1h	PROPN
admet-249	89	16	)	)	PUNCT
admet-249	89	17	and	and	CCONJ
admet-249	89	18	two	two	NUM
admet-249	89	19	-	-	PUNCT
admet-249	89	20	dimensional	dimensional	ADJ
admet-249	89	21	nmr	nmr	NOUN
admet-249	89	22	spectra	spectra	NOUN
admet-249	89	23	(	(	PUNCT
admet-249	89	24	cosy	cosy	NOUN
admet-249	89	25	,	,	PUNCT
admet-249	89	26	hsqc	hsqc	NOUN
admet-249	89	27	and	and	CCONJ
admet-249	89	28	hmbc	hmbc	PROPN
admet-249	89	29	)	)	PUNCT
admet-249	89	30	.	.	PUNCT
admet-249	90	1	admet	admet	PROPN
admet-249	90	2	&	&	CCONJ
admet-249	90	3	dmpk	dmpk	PROPN
admet-249	90	4	3(4	3(4	NUM
admet-249	90	5	)	)	PUNCT
admet-249	90	6	(	(	PUNCT
admet-249	90	7	2015	2015	NUM
admet-249	90	8	)	)	PUNCT
admet-249	90	9	352	352	NUM
admet-249	90	10	-	-	SYM
admet-249	90	11	358	358	NUM
admet-249	90	12	carbohydrazide	carbohydrazide	ADJ
admet-249	90	13	reaction	reaction	NOUN
admet-249	90	14	monitoring	monitoring	NOUN
admet-249	90	15	by	by	ADP
admet-249	90	16	lc	lc	PROPN
admet-249	90	17	-	-	PUNCT
admet-249	90	18	dad	dad	NOUN
admet-249	90	19	-	-	PUNCT
admet-249	90	20	spe	spe	PROPN
admet-249	90	21	-	-	PUNCT
admet-249	90	22	nmr	nmr	NOUN
admet-249	90	23	doi	doi	NOUN
admet-249	90	24	:	:	PUNCT
admet-249	90	25	10.5599	10.5599	NUM
admet-249	90	26	/	/	SYM
admet-249	90	27	admet.3.4.249	admet.3.4.249	NOUN
admet-249	90	28	357	357	NUM
admet-249	90	29	figure	figure	NOUN
admet-249	90	30	4	4	NUM
admet-249	90	31	.	.	PUNCT
admet-249	90	32	cosy	cosy	PROPN
admet-249	90	33	nmr	nmr	NOUN
admet-249	90	34	spectrum	spectrum	NOUN
admet-249	90	35	obtained	obtain	VERB
admet-249	90	36	in	in	ADP
admet-249	90	37	lc	lc	PROPN
admet-249	90	38	-	-	PUNCT
admet-249	90	39	spe	spe	NOUN
admet-249	90	40	-	-	PUNCT
admet-249	90	41	nmr	nmr	NOUN
admet-249	90	42	mode	mode	NOUN
admet-249	90	43	for	for	ADP
admet-249	90	44	iv	iv	NUM
admet-249	90	45	isolated	isolate	VERB
admet-249	90	46	from	from	ADP
admet-249	90	47	the	the	DET
admet-249	90	48	reaction	reaction	NOUN
admet-249	90	49	mixture	mixture	NOUN
admet-249	90	50	(	(	PUNCT
admet-249	90	51	16	16	NUM
admet-249	90	52	scans	scan	NOUN
admet-249	90	53	,	,	PUNCT
admet-249	90	54	1h	1h	NUM
admet-249	90	55	and	and	CCONJ
admet-249	90	56	16	16	NUM
admet-249	90	57	min	min	NOUN
admet-249	90	58	)	)	PUNCT
admet-249	90	59	.	.	PUNCT
admet-249	91	1	conclusions	conclusion	NOUN
admet-249	91	2	condensation	condensation	NOUN
admet-249	91	3	reaction	reaction	NOUN
admet-249	91	4	of	of	ADP
admet-249	91	5	carbohydrazide	carbohydrazide	NOUN
admet-249	91	6	with	with	ADP
admet-249	91	7	salicylaldehyde	salicylaldehyde	NOUN
admet-249	91	8	was	be	AUX
admet-249	91	9	successfully	successfully	ADV
admet-249	91	10	monitored	monitor	VERB
admet-249	91	11	by	by	ADP
admet-249	91	12	lc	lc	NOUN
admet-249	91	13	-	-	PUNCT
admet-249	91	14	dadspe	dadspe	PROPN
admet-249	91	15	-	-	PUNCT
admet-249	91	16	nmr	nmr	NOUN
admet-249	91	17	with	with	ADP
admet-249	91	18	prodigy	prodigy	NOUN
admet-249	91	19	cryoprobe	cryoprobe	NOUN
admet-249	91	20	.	.	PUNCT
admet-249	92	1	application	application	NOUN
admet-249	92	2	of	of	ADP
admet-249	92	3	this	this	DET
admet-249	92	4	method	method	NOUN
admet-249	92	5	made	make	VERB
admet-249	92	6	it	it	PRON
admet-249	92	7	possible	possible	ADJ
admet-249	92	8	to	to	PART
admet-249	92	9	identify	identify	VERB
admet-249	92	10	and	and	CCONJ
admet-249	92	11	structurally	structurally	ADV
admet-249	92	12	characterise	characterise	VERB
admet-249	92	13	reaction	reaction	NOUN
admet-249	92	14	products	product	NOUN
admet-249	92	15	in	in	ADP
admet-249	92	16	a	a	DET
admet-249	92	17	fast	fast	ADJ
admet-249	92	18	and	and	CCONJ
admet-249	92	19	efficient	efficient	ADJ
admet-249	92	20	manner	manner	NOUN
admet-249	92	21	.	.	PUNCT
admet-249	93	1	after	after	SCONJ
admet-249	93	2	the	the	DET
admet-249	93	3	reaction	reaction	NOUN
admet-249	93	4	mixture	mixture	NOUN
admet-249	93	5	components	component	NOUN
admet-249	93	6	were	be	AUX
admet-249	93	7	separated	separate	VERB
admet-249	93	8	on	on	ADP
admet-249	93	9	the	the	DET
admet-249	93	10	chromatographic	chromatographic	ADJ
admet-249	93	11	column	column	NOUN
admet-249	93	12	and	and	CCONJ
admet-249	93	13	trapped	trap	VERB
admet-249	93	14	on	on	ADP
admet-249	93	15	spe	spe	PROPN
admet-249	93	16	cartridges	cartridge	NOUN
admet-249	93	17	,	,	PUNCT
admet-249	93	18	they	they	PRON
admet-249	93	19	were	be	AUX
admet-249	93	20	sent	send	VERB
admet-249	93	21	to	to	ADP
admet-249	93	22	nmr	nmr	NOUN
admet-249	93	23	.	.	PUNCT
admet-249	94	1	one	one	NUM
admet-249	94	2	and	and	CCONJ
admet-249	94	3	two	two	NUM
admet-249	94	4	-	-	PUNCT
admet-249	94	5	dimensional	dimensional	ADJ
admet-249	94	6	nmr	nmr	NOUN
admet-249	94	7	spectra	spectra	NOUN
admet-249	94	8	were	be	AUX
admet-249	94	9	recorded	record	VERB
admet-249	94	10	and	and	CCONJ
admet-249	94	11	analysed	analyse	VERB
admet-249	94	12	.	.	PUNCT
admet-249	95	1	spectral	spectral	ADJ
admet-249	95	2	analysis	analysis	NOUN
admet-249	95	3	confirmed	confirm	VERB
admet-249	95	4	the	the	DET
admet-249	95	5	structures	structure	NOUN
admet-249	95	6	of	of	ADP
admet-249	95	7	the	the	DET
admet-249	95	8	reaction	reaction	NOUN
admet-249	95	9	products	product	NOUN
admet-249	95	10	,	,	PUNCT
admet-249	95	11	e.g.	e.g.	ADV
admet-249	95	12	mono(iii	mono(iii	NOUN
admet-249	95	13	)	)	PUNCT
admet-249	95	14	and	and	CCONJ
admet-249	95	15	bis(salicylidene)carbohydrazide	bis(salicylidene)carbohydrazide	NUM
admet-249	95	16	(	(	PUNCT
admet-249	95	17	iv	iv	X
admet-249	95	18	)	)	PUNCT
admet-249	95	19	.	.	PUNCT
admet-249	96	1	references	reference	NOUN
admet-249	96	2	[	[	X
admet-249	96	3	1	1	X
admet-249	96	4	]	]	PUNCT
admet-249	96	5	s.	s.	PROPN
admet-249	96	6	barman	barman	PROPN
admet-249	96	7	,	,	PUNCT
admet-249	96	8	l.	l.	PROPN
admet-249	96	9	you	you	PRON
admet-249	96	10	,	,	PUNCT
admet-249	96	11	r.	r.	PROPN
admet-249	96	12	chen	chen	PROPN
admet-249	96	13	,	,	PUNCT
admet-249	96	14	v.	v.	ADP
admet-249	96	15	codrea	codrea	PROPN
admet-249	96	16	,	,	PUNCT
admet-249	96	17	g.	g.	PROPN
admet-249	96	18	kago	kago	PROPN
admet-249	96	19	,	,	PUNCT
admet-249	96	20	r.	r.	PROPN
admet-249	96	21	edupuganti	edupuganti	PROPN
admet-249	96	22	,	,	PUNCT
admet-249	96	23	j.	j.	PROPN
admet-249	96	24	robertus	robertus	PROPN
admet-249	96	25	,	,	PUNCT
admet-249	96	26	r.m	r.m	PROPN
admet-249	96	27	.	.	PROPN
admet-249	96	28	krug	krug	PROPN
admet-249	96	29	,	,	PUNCT
admet-249	96	30	e.	e.	PROPN
admet-249	96	31	v.	v.	PROPN
admet-249	96	32	anslyn	anslyn	PROPN
admet-249	96	33	,	,	PUNCT
admet-249	96	34	european	european	PROPN
admet-249	96	35	journal	journal	PROPN
admet-249	96	36	of	of	ADP
admet-249	96	37	medicinal	medicinal	ADJ
admet-249	96	38	chemistry	chemistry	NOUN
admet-249	96	39	71	71	NUM
admet-249	96	40	(	(	PUNCT
admet-249	96	41	2014	2014	NUM
admet-249	96	42	)	)	PUNCT
admet-249	96	43	81	81	NUM
admet-249	96	44	-	-	SYM
admet-249	96	45	90	90	NUM
admet-249	96	46	.	.	PUNCT
admet-249	97	1	[	[	X
admet-249	97	2	2	2	X
admet-249	97	3	]	]	X
admet-249	97	4	v.n	v.n	PROPN
admet-249	97	5	.	.	PROPN
admet-249	97	6	telvekar	telvekar	PROPN
admet-249	97	7	,	,	PUNCT
admet-249	97	8	a.	a.	PROPN
admet-249	97	9	belubbi	belubbi	PROPN
admet-249	97	10	,	,	PUNCT
admet-249	97	11	v.k	v.k	PROPN
admet-249	97	12	.	.	PROPN
admet-249	97	13	bairwa	bairwa	PROPN
admet-249	97	14	,	,	PUNCT
admet-249	97	15	k.	k.	PROPN
admet-249	97	16	satardekar	satardekar	PROPN
admet-249	97	17	,	,	PUNCT
admet-249	97	18	bioorganic	bioorganic	PROPN
admet-249	97	19	&	&	CCONJ
admet-249	97	20	medicinal	medicinal	ADJ
admet-249	97	21	chemistry	chemistry	NOUN
admet-249	97	22	letters	letter	NOUN
admet-249	97	23	22	22	NUM
admet-249	97	24	(	(	PUNCT
admet-249	97	25	2012	2012	NUM
admet-249	97	26	)	)	PUNCT
admet-249	97	27	2343	2343	NUM
admet-249	97	28	-	-	SYM
admet-249	97	29	2346	2346	NUM
admet-249	97	30	.	.	PUNCT
admet-249	98	1	[	[	X
admet-249	98	2	3	3	X
admet-249	98	3	]	]	PUNCT
admet-249	98	4	t.	t.	PROPN
admet-249	98	5	aboul	aboul	NOUN
admet-249	98	6	-	-	NOUN
admet-249	98	7	fadl	fadl	ADJ
admet-249	98	8	,	,	PUNCT
admet-249	98	9	f.a.s	f.a.s	NOUN
admet-249	98	10	.	.	PUNCT
admet-249	99	1	bin	bin	NOUN
admet-249	99	2	-	-	NOUN
admet-249	99	3	jubair	jubair	NOUN
admet-249	99	4	,	,	PUNCT
admet-249	99	5	o.	o.	PROPN
admet-249	99	6	aboul	aboul	PROPN
admet-249	99	7	-	-	PUNCT
admet-249	99	8	wafa	wafa	PROPN
admet-249	99	9	,	,	PUNCT
admet-249	99	10	european	european	ADJ
admet-249	99	11	journal	journal	PROPN
admet-249	99	12	of	of	ADP
admet-249	99	13	medicinal	medicinal	ADJ
admet-249	99	14	chemistry	chemistry	NOUN
admet-249	99	15	45	45	NUM
admet-249	99	16	(	(	PUNCT
admet-249	99	17	2010	2010	NUM
admet-249	99	18	)	)	PUNCT
admet-249	99	19	4578	4578	NUM
admet-249	99	20	-	-	SYM
admet-249	99	21	4586	4586	NUM
admet-249	99	22	.	.	PUNCT
admet-249	100	1	[	[	X
admet-249	100	2	4	4	X
admet-249	100	3	]	]	PUNCT
admet-249	100	4	j.	j.	PROPN
admet-249	100	5	camacho	camacho	PROPN
admet-249	100	6	,	,	PUNCT
admet-249	100	7	a.	a.	NOUN
admet-249	100	8	barazarte	barazarte	NOUN
admet-249	100	9	,	,	PUNCT
admet-249	100	10	n.	n.	PROPN
admet-249	100	11	gamboa	gamboa	PROPN
admet-249	100	12	,	,	PUNCT
admet-249	100	13	j.	j.	PROPN
admet-249	100	14	rodrigues	rodrigues	PROPN
admet-249	100	15	,	,	PUNCT
admet-249	100	16	r.	r.	PROPN
admet-249	100	17	rojas	rojas	PROPN
admet-249	100	18	,	,	PUNCT
admet-249	100	19	a.	a.	PROPN
admet-249	100	20	vaisberg	vaisberg	PROPN
admet-249	100	21	,	,	PUNCT
admet-249	100	22	r.	r.	PROPN
admet-249	100	23	gilman	gilman	PROPN
admet-249	100	24	,	,	PUNCT
admet-249	100	25	j.	j.	PROPN
admet-249	100	26	charris	charris	PROPN
admet-249	100	27	,	,	PUNCT
admet-249	100	28	bioorganic	bioorganic	PROPN
admet-249	100	29	&	&	CCONJ
admet-249	100	30	medicinal	medicinal	ADJ
admet-249	100	31	chemistry	chemistry	NOUN
admet-249	100	32	19	19	NUM
admet-249	100	33	(	(	PUNCT
admet-249	100	34	2011	2011	NUM
admet-249	100	35	)	)	PUNCT
admet-249	100	36	2023	2023	NUM
admet-249	100	37	-	-	SYM
admet-249	100	38	2029	2029	NUM
admet-249	100	39	.	.	PUNCT
admet-249	101	1	[	[	X
admet-249	101	2	5	5	X
admet-249	101	3	]	]	X
admet-249	101	4	a.h	a.h	PROPN
admet-249	101	5	.	.	PROPN
admet-249	101	6	corvin	corvin	PROPN
admet-249	101	7	,	,	PUNCT
admet-249	101	8	j.d	j.d	PROPN
admet-249	101	9	.	.	PROPN
admet-249	101	10	reinheimer	reinheimer	NOUN
admet-249	101	11	,	,	PUNCT
admet-249	101	12	journal	journal	NOUN
admet-249	101	13	of	of	ADP
admet-249	101	14	american	american	PROPN
admet-249	101	15	chemical	chemical	PROPN
admet-249	101	16	society	society	PROPN
admet-249	101	17	73(3	73(3	NUM
admet-249	101	18	)	)	PUNCT
admet-249	101	19	(	(	PUNCT
admet-249	101	20	1951	1951	NUM
admet-249	101	21	)	)	PUNCT
admet-249	101	22	1184	1184	NUM
admet-249	101	23	-	-	SYM
admet-249	101	24	1186	1186	NUM
admet-249	101	25	.	.	PUNCT
admet-249	102	1	[	[	X
admet-249	102	2	6	6	NUM
admet-249	102	3	]	]	X
admet-249	102	4	b.f	b.f	PROPN
admet-249	102	5	.	.	PROPN
admet-249	102	6	abdel	abdel	PROPN
admet-249	102	7	-	-	PUNCT
admet-249	102	8	wahab	wahab	PROPN
admet-249	102	9	,	,	PUNCT
admet-249	102	10	a.-a	a.-a	PROPN
admet-249	102	11	.	.	PUNCT
admet-249	103	1	s.	s.	PROPN
admet-249	103	2	el	el	PROPN
admet-249	103	3	-	-	PUNCT
admet-249	103	4	ahl	ahl	PROPN
admet-249	103	5	,	,	PUNCT
admet-249	103	6	phosphorus	phosphorus	NOUN
admet-249	103	7	,	,	PUNCT
admet-249	103	8	sulfur	sulfur	NOUN
admet-249	103	9	,	,	PUNCT
admet-249	103	10	and	and	CCONJ
admet-249	103	11	silicon	silicon	NOUN
admet-249	103	12	,	,	PUNCT
admet-249	103	13	185	185	NUM
admet-249	103	14	(	(	PUNCT
admet-249	103	15	2010	2010	NUM
admet-249	103	16	)	)	PUNCT
admet-249	103	17	249	249	NUM
admet-249	103	18	-	-	SYM
admet-249	103	19	260	260	NUM
admet-249	103	20	.	.	PUNCT
admet-249	104	1	[	[	X
admet-249	104	2	7	7	X
admet-249	104	3	]	]	X
admet-249	104	4	m.	m.	NOUN
admet-249	104	5	sutradhar	sutradhar	PROPN
admet-249	104	6	,	,	PUNCT
admet-249	104	7	t.	t.	PROPN
admet-249	104	8	r.	r.	PROPN
admet-249	104	9	barman	barman	PROPN
admet-249	104	10	,	,	PUNCT
admet-249	104	11	e.	e.	PROPN
admet-249	104	12	rentschler	rentschler	PROPN
admet-249	104	13	,	,	PUNCT
admet-249	104	14	inorganic	inorganic	ADJ
admet-249	104	15	chemistry	chemistry	NOUN
admet-249	104	16	communications	communication	NOUN
admet-249	104	17	39	39	NUM
admet-249	104	18	(	(	PUNCT
admet-249	104	19	2014	2014	NUM
admet-249	104	20	)	)	PUNCT
admet-249	104	21	140	140	NUM
admet-249	104	22	-	-	SYM
admet-249	104	23	143	143	NUM
admet-249	104	24	.	.	PUNCT
admet-249	105	1	[	[	X
admet-249	105	2	8	8	NUM
admet-249	105	3	]	]	X
admet-249	105	4	r.	r.	PROPN
admet-249	105	5	n.	n.	PROPN
admet-249	105	6	patel	patel	PROPN
admet-249	105	7	,	,	PUNCT
admet-249	105	8	inorganica	inorganica	PROPN
admet-249	105	9	chimica	chimica	PROPN
admet-249	105	10	acta	acta	PROPN
admet-249	105	11	363	363	NUM
admet-249	105	12	(	(	PUNCT
admet-249	105	13	2010	2010	NUM
admet-249	105	14	)	)	PUNCT
admet-249	105	15	3838	3838	NUM
admet-249	105	16	-	-	SYM
admet-249	105	17	3846	3846	NUM
admet-249	105	18	.	.	PUNCT
admet-249	106	1	[	[	X
admet-249	106	2	9	9	NUM
admet-249	106	3	]	]	PUNCT
admet-249	106	4	p.	p.	NOUN
admet-249	106	5	novak	novak	PROPN
admet-249	106	6	,	,	PUNCT
admet-249	106	7	t.	t.	PROPN
admet-249	106	8	jednačak	jednačak	PROPN
admet-249	106	9	,	,	PUNCT
admet-249	106	10	j.	j.	PROPN
admet-249	106	11	parlov	parlov	PROPN
admet-249	106	12	vuković	vuković	PROPN
admet-249	106	13	,	,	PUNCT
admet-249	106	14	k.	k.	PROPN
admet-249	106	15	zangger	zangger	PROPN
admet-249	106	16	,	,	PUNCT
admet-249	106	17	m.	m.	NOUN
admet-249	106	18	rubčić	rubčić	PROPN
admet-249	106	19	,	,	PUNCT
admet-249	106	20	n.	n.	NOUN
admet-249	106	21	galić	galić	NOUN
admet-249	106	22	,	,	PUNCT
admet-249	106	23	t.	t.	PROPN
admet-249	106	24	hrenar	hrenar	PROPN
admet-249	106	25	,	,	PUNCT
admet-249	106	26	croatica	croatica	PROPN
admet-249	106	27	chemica	chemica	PROPN
admet-249	106	28	acta	acta	PROPN
admet-249	106	29	85	85	NUM
admet-249	106	30	(	(	PUNCT
admet-249	106	31	4	4	NUM
admet-249	106	32	)	)	PUNCT
admet-249	106	33	(	(	PUNCT
admet-249	106	34	2012	2012	NUM
admet-249	106	35	)	)	PUNCT
admet-249	106	36	451	451	NUM
admet-249	106	37	-	-	SYM
admet-249	106	38	456	456	NUM
admet-249	106	39	.	.	PUNCT
admet-249	107	1	habinovec	habinovec	PROPN
admet-249	107	2	et	et	PROPN
admet-249	107	3	al	al	PROPN
admet-249	107	4	.	.	PROPN
admet-249	107	5	admet	admet	PROPN
admet-249	107	6	&	&	CCONJ
admet-249	107	7	dmpk	dmpk	PROPN
admet-249	107	8	3(4	3(4	NUM
admet-249	107	9	)	)	PUNCT
admet-249	107	10	(	(	PUNCT
admet-249	107	11	2015	2015	NUM
admet-249	107	12	)	)	PUNCT
admet-249	107	13	352	352	NUM
admet-249	107	14	-	-	SYM
admet-249	107	15	358	358	NUM
admet-249	107	16	358	358	NUM
admet-249	108	1	[	[	X
admet-249	108	2	10	10	NUM
admet-249	108	3	]	]	PUNCT
admet-249	108	4	m.	m.	NOUN
admet-249	108	5	rubčić	rubčić	NOUN
admet-249	108	6	,	,	PUNCT
admet-249	108	7	n.	n.	NOUN
admet-249	108	8	galić	galić	NOUN
admet-249	108	9	,	,	PUNCT
admet-249	108	10	i.	i.	PROPN
admet-249	108	11	halasz	halasz	PROPN
admet-249	108	12	,	,	PUNCT
admet-249	108	13	t.	t.	PROPN
admet-249	108	14	jednačak	jednačak	PROPN
admet-249	108	15	,	,	PUNCT
admet-249	108	16	n.	n.	PROPN
admet-249	108	17	judaš	judaš	PROPN
admet-249	108	18	,	,	PUNCT
admet-249	108	19	j.	j.	PROPN
admet-249	108	20	plavec	plavec	PROPN
admet-249	108	21	,	,	PUNCT
admet-249	108	22	p.	p.	NOUN
admet-249	108	23	šket	šket	NOUN
admet-249	108	24	,	,	PUNCT
admet-249	108	25	p.	p.	PROPN
admet-249	108	26	novak	novak	PROPN
admet-249	108	27	,	,	PUNCT
admet-249	108	28	crystal	crystal	NOUN
admet-249	108	29	growth	growth	PROPN
admet-249	108	30	&	&	CCONJ
admet-249	108	31	design	design	PROPN
admet-249	108	32	14	14	NUM
admet-249	108	33	(	(	PUNCT
admet-249	108	34	2014	2014	NUM
admet-249	108	35	)	)	PUNCT
admet-249	108	36	2900	2900	NUM
admet-249	108	37	-	-	SYM
admet-249	108	38	2912	2912	NUM
admet-249	108	39	.	.	PUNCT
admet-249	109	1	[	[	X
admet-249	109	2	11	11	NUM
admet-249	109	3	]	]	PUNCT
admet-249	109	4	t.	t.	PROPN
admet-249	109	5	jednačak	jednačak	PROPN
admet-249	109	6	,	,	PUNCT
admet-249	109	7	p.	p.	PROPN
admet-249	109	8	novak	novak	PROPN
admet-249	109	9	,	,	PUNCT
admet-249	109	10	a.	a.	NOUN
admet-249	109	11	hodzic	hodzic	NOUN
admet-249	109	12	,	,	PUNCT
admet-249	109	13	o.	o.	NOUN
admet-249	109	14	scheibelhofer	scheibelhofer	PROPN
admet-249	109	15	,	,	PUNCT
admet-249	109	16	j.	j.	PROPN
admet-249	109	17	g.	g.	PROPN
admet-249	109	18	khinast	khinast	PROPN
admet-249	109	19	,	,	PUNCT
admet-249	109	20	j.	j.	PROPN
admet-249	109	21	plavec	plavec	PROPN
admet-249	109	22	,	,	PUNCT
admet-249	109	23	p.	p.	PROPN
admet-249	109	24	šket	šket	NOUN
admet-249	109	25	,	,	PUNCT
admet-249	109	26	j.	j.	PROPN
admet-249	109	27	parlov	parlov	PROPN
admet-249	109	28	vuković	vuković	PROPN
admet-249	109	29	,	,	PUNCT
admet-249	109	30	acta	acta	PROPN
admet-249	109	31	chimica	chimica	PROPN
admet-249	109	32	slovenica	slovenica	PROPN
admet-249	109	33	61	61	NUM
admet-249	109	34	(	(	PUNCT
admet-249	109	35	2014	2014	NUM
admet-249	109	36	)	)	PUNCT
admet-249	109	37	161	161	NUM
admet-249	109	38	-	-	SYM
admet-249	109	39	169	169	NUM
admet-249	109	40	.	.	PUNCT
admet-249	110	1	[	[	X
admet-249	110	2	12	12	NUM
admet-249	110	3	]	]	X
admet-249	110	4	s.	s.	PROPN
admet-249	110	5	görög	görög	PROPN
admet-249	110	6	,	,	PUNCT
admet-249	110	7	trends	trend	NOUN
admet-249	110	8	in	in	ADP
admet-249	110	9	analytical	analytical	ADJ
admet-249	110	10	chemistry	chemistry	NOUN
admet-249	110	11	69	69	NUM
admet-249	110	12	(	(	PUNCT
admet-249	110	13	2015	2015	NUM
admet-249	110	14	)	)	PUNCT
admet-249	110	15	114	114	NUM
admet-249	110	16	-	-	SYM
admet-249	110	17	122	122	NUM
admet-249	110	18	.	.	PUNCT
admet-249	111	1	[	[	X
admet-249	111	2	13	13	NUM
admet-249	111	3	]	]	PUNCT
admet-249	111	4	p.	p.	PROPN
admet-249	111	5	novak	novak	PROPN
admet-249	111	6	,	,	PUNCT
admet-249	111	7	m.	m.	NOUN
admet-249	111	8	cindrić	cindrić	NOUN
admet-249	111	9	,	,	PUNCT
admet-249	111	10	p.	p.	NOUN
admet-249	111	11	tepeš	tepeš	NOUN
admet-249	111	12	,	,	PUNCT
admet-249	111	13	s.	s.	PROPN
admet-249	111	14	dragojević	dragojević	PROPN
admet-249	111	15	,	,	PUNCT
admet-249	111	16	m.	m.	NOUN
admet-249	111	17	ilijaš	ilijaš	PROPN
admet-249	111	18	,	,	PUNCT
admet-249	111	19	k.	k.	PROPN
admet-249	111	20	mihaljević	mihaljević	PROPN
admet-249	111	21	,	,	PUNCT
admet-249	111	22	journal	journal	NOUN
admet-249	111	23	of	of	ADP
admet-249	111	24	separation	separation	NOUN
admet-249	111	25	science	science	NOUN
admet-249	111	26	28	28	NUM
admet-249	111	27	(	(	PUNCT
admet-249	111	28	2005	2005	NUM
admet-249	111	29	)	)	PUNCT
admet-249	111	30	1442	1442	NUM
admet-249	111	31	-	-	SYM
admet-249	111	32	1447	1447	NUM
admet-249	111	33	.	.	PUNCT
admet-249	112	1	[	[	X
admet-249	112	2	14	14	NUM
admet-249	112	3	]	]	X
admet-249	112	4	s.	s.	PROPN
admet-249	112	5	singh	singh	PROPN
admet-249	112	6	,	,	PUNCT
admet-249	112	7	t.	t.	PROPN
admet-249	112	8	handa	handa	PROPN
admet-249	112	9	,	,	PUNCT
admet-249	112	10	m.	m.	NOUN
admet-249	112	11	narayanam	narayanam	PROPN
admet-249	112	12	,	,	PUNCT
admet-249	112	13	a.	a.	PROPN
admet-249	112	14	sahu	sahu	PROPN
admet-249	112	15	,	,	PUNCT
admet-249	112	16	m.	m.	NOUN
admet-249	112	17	junwal	junwal	PROPN
admet-249	112	18	,	,	PUNCT
admet-249	112	19	r.	r.	PROPN
admet-249	112	20	p.	p.	PROPN
admet-249	112	21	shah	shah	PROPN
admet-249	112	22	,	,	PUNCT
admet-249	112	23	journal	journal	NOUN
admet-249	112	24	of	of	ADP
admet-249	112	25	pharmaceutical	pharmaceutical	NOUN
admet-249	112	26	and	and	CCONJ
admet-249	112	27	biomedical	biomedical	ADJ
admet-249	112	28	anaysis	anaysis	NOUN
admet-249	112	29	69	69	NUM
admet-249	112	30	(	(	PUNCT
admet-249	112	31	2012	2012	NUM
admet-249	112	32	)	)	PUNCT
admet-249	112	33	148	148	NUM
admet-249	112	34	-	-	SYM
admet-249	112	35	173	173	NUM
admet-249	112	36	.	.	PUNCT
admet-249	113	1	[	[	X
admet-249	113	2	15	15	NUM
admet-249	113	3	]	]	X
admet-249	113	4	p.	p.	NOUN
admet-249	113	5	novak	novak	PROPN
admet-249	113	6	,	,	PUNCT
admet-249	113	7	p.	p.	NOUN
admet-249	113	8	tepeš	tepeš	NOUN
admet-249	113	9	,	,	PUNCT
admet-249	113	10	m.	m.	NOUN
admet-249	113	11	cindrić	cindrić	NOUN
admet-249	113	12	,	,	PUNCT
admet-249	113	13	m.	m.	NOUN
admet-249	113	14	ilijaš	ilijaš	PROPN
admet-249	113	15	,	,	PUNCT
admet-249	113	16	s.	s.	PROPN
admet-249	113	17	dragojević	dragojević	PROPN
admet-249	113	18	,	,	PUNCT
admet-249	113	19	k.	k.	PROPN
admet-249	113	20	mihaljević	mihaljević	PROPN
admet-249	113	21	,	,	PUNCT
admet-249	113	22	journal	journal	NOUN
admet-249	113	23	of	of	ADP
admet-249	113	24	chromatography	chromatography	NOUN
admet-249	113	25	a	a	DET
admet-249	113	26	1033	1033	NUM
admet-249	113	27	(	(	PUNCT
admet-249	113	28	2004	2004	NUM
admet-249	113	29	)	)	PUNCT
admet-249	113	30	,	,	PUNCT
admet-249	113	31	299	299	NUM
admet-249	113	32	-	-	SYM
admet-249	113	33	303	303	NUM
admet-249	113	34	.	.	PUNCT
admet-249	114	1	[	[	X
admet-249	114	2	16	16	NUM
admet-249	114	3	]	]	PUNCT
admet-249	114	4	p.	p.	PROPN
admet-249	114	5	novak	novak	PROPN
admet-249	114	6	,	,	PUNCT
admet-249	114	7	p.	p.	NOUN
admet-249	114	8	tepeš	tepeš	NOUN
admet-249	114	9	,	,	PUNCT
admet-249	114	10	m.	m.	NOUN
admet-249	114	11	ilijaš	ilijaš	PROPN
admet-249	114	12	,	,	PUNCT
admet-249	114	13	i.	i.	PROPN
admet-249	114	14	fistrić	fistrić	PROPN
admet-249	114	15	,	,	PUNCT
admet-249	114	16	i.	i.	NOUN
admet-249	114	17	bratoš	bratoš	PROPN
admet-249	114	18	,	,	PUNCT
admet-249	114	19	a.	a.	NOUN
admet-249	114	20	avdagić	avdagić	ADV
admet-249	114	21	,	,	PUNCT
admet-249	114	22	v.	v.	ADP
admet-249	114	23	gabelica	gabelica	PROPN
admet-249	114	24	marković	marković	PROPN
admet-249	114	25	,	,	PUNCT
admet-249	114	26	m.	m.	NOUN
admet-249	114	27	dumić	dumić	PROPN
admet-249	114	28	,	,	PUNCT
admet-249	114	29	journal	journal	NOUN
admet-249	114	30	of	of	ADP
admet-249	114	31	pharmaceutical	pharmaceutical	NOUN
admet-249	114	32	and	and	CCONJ
admet-249	114	33	biomedical	biomedical	ADJ
admet-249	114	34	anaysis	anaysis	NOUN
admet-249	114	35	50	50	NUM
admet-249	114	36	(	(	PUNCT
admet-249	114	37	2009	2009	NUM
admet-249	114	38	)	)	PUNCT
admet-249	114	39	68	68	NUM
admet-249	114	40	-	-	SYM
admet-249	114	41	72	72	NUM
admet-249	114	42	.	.	PUNCT
admet-249	115	1	[	[	X
admet-249	115	2	17	17	NUM
admet-249	115	3	]	]	X
admet-249	115	4	g.	g.	PROPN
admet-249	115	5	schlotterbeck	schlotterbeck	PROPN
admet-249	115	6	,	,	PUNCT
admet-249	115	7	s.m	s.m	PROPN
admet-249	115	8	.	.	PROPN
admet-249	115	9	ceccarelli	ceccarelli	PROPN
admet-249	115	10	,	,	PUNCT
admet-249	115	11	bioanalysis	bioanalysis	NOUN
admet-249	115	12	1	1	NUM
admet-249	115	13	(	(	PUNCT
admet-249	115	14	2009	2009	NUM
admet-249	115	15	)	)	PUNCT
admet-249	115	16	549	549	NUM
admet-249	115	17	-	-	SYM
admet-249	115	18	559	559	NUM
admet-249	115	19	.	.	PUNCT
admet-249	116	1	[	[	X
admet-249	116	2	18	18	NUM
admet-249	116	3	]	]	X
admet-249	116	4	s.	s.	PROPN
admet-249	116	5	sturm	sturm	PROPN
admet-249	116	6	,	,	PUNCT
admet-249	116	7	c.	c.	PROPN
admet-249	116	8	seger	seger	PROPN
admet-249	116	9	,	,	PUNCT
admet-249	116	10	journal	journal	NOUN
admet-249	116	11	of	of	ADP
admet-249	116	12	chromatography	chromatography	NOUN
admet-249	116	13	a	a	DET
admet-249	116	14	1259	1259	NUM
admet-249	116	15	(	(	PUNCT
admet-249	116	16	2012	2012	NUM
admet-249	116	17	)	)	PUNCT
admet-249	116	18	50	50	NUM
admet-249	116	19	-	-	SYM
admet-249	116	20	61	61	NUM
admet-249	116	21	.	.	PUNCT
admet-249	117	1	[	[	X
admet-249	117	2	19	19	NUM
admet-249	117	3	]	]	PUNCT
admet-249	117	4	j.	j.	PROPN
admet-249	117	5	w.	w.	PROPN
admet-249	117	6	jaroszewski	jaroszewski	PROPN
admet-249	117	7	,	,	PUNCT
admet-249	117	8	planta	planta	NOUN
admet-249	117	9	medica	medica	NOUN
admet-249	117	10	71	71	NUM
admet-249	117	11	(	(	PUNCT
admet-249	117	12	2005	2005	NUM
admet-249	117	13	)	)	PUNCT
admet-249	117	14	795	795	NUM
admet-249	117	15	-	-	SYM
admet-249	117	16	802	802	NUM
admet-249	117	17	.	.	PUNCT
admet-249	118	1	[	[	X
admet-249	118	2	20	20	NUM
admet-249	118	3	]	]	PUNCT
admet-249	118	4	s.	s.	PROPN
admet-249	118	5	schmidt	schmidt	PROPN
admet-249	118	6	,	,	PUNCT
admet-249	118	7	c.	c.	PROPN
admet-249	118	8	piechotta	piechotta	NOUN
admet-249	118	9	,	,	PUNCT
admet-249	118	10	m.	m.	NOUN
admet-249	118	11	godejohann	godejohann	PROPN
admet-249	118	12	,	,	PUNCT
admet-249	118	13	i.	i.	NOUN
admet-249	118	14	nihels	nihels	PROPN
admet-249	118	15	,	,	PUNCT
admet-249	118	16	c.	c.	PROPN
admet-249	118	17	mügge	mügge	PROPN
admet-249	118	18	,	,	PUNCT
admet-249	118	19	talanta	talanta	ADJ
admet-249	118	20	,	,	PUNCT
admet-249	118	21	82	82	NUM
admet-249	118	22	(	(	PUNCT
admet-249	118	23	2010	2010	NUM
admet-249	118	24	)	)	PUNCT
admet-249	118	25	143	143	NUM
admet-249	118	26	-	-	SYM
admet-249	118	27	150	150	NUM
admet-249	118	28	.	.	PUNCT
admet-249	119	1	[	[	X
admet-249	119	2	21	21	NUM
admet-249	119	3	]	]	X
admet-249	119	4	s.	s.	PROPN
admet-249	119	5	christophoridou	christophoridou	PROPN
admet-249	119	6	,	,	PUNCT
admet-249	119	7	p.	p.	NOUN
admet-249	119	8	dais	dais	PROPN
admet-249	119	9	,	,	PUNCT
admet-249	119	10	l.	l.	PROPN
admet-249	119	11	h.	h.	PROPN
admet-249	119	12	tseng	tseng	PROPN
admet-249	119	13	,	,	PUNCT
admet-249	119	14	m.	m.	NOUN
admet-249	119	15	spraul	spraul	PROPN
admet-249	119	16	,	,	PUNCT
admet-249	119	17	journal	journal	NOUN
admet-249	119	18	of	of	ADP
admet-249	119	19	agriultural	agriultural	ADJ
admet-249	119	20	and	and	CCONJ
admet-249	119	21	food	food	NOUN
admet-249	119	22	chemistry	chemistry	NOUN
admet-249	119	23	53	53	NUM
admet-249	119	24	(	(	PUNCT
admet-249	119	25	2005	2005	NUM
admet-249	119	26	)	)	PUNCT
admet-249	119	27	4667	4667	NUM
admet-249	119	28	-	-	SYM
admet-249	119	29	4679	4679	NUM
admet-249	119	30	.	.	PUNCT
admet-249	120	1	[	[	X
admet-249	120	2	22	22	NUM
admet-249	120	3	]	]	PUNCT
admet-249	120	4	c.	c.	NOUN
admet-249	120	5	seger	seger	PROPN
admet-249	120	6	,	,	PUNCT
admet-249	120	7	m.	m.	NOUN
admet-249	120	8	godejohann	godejohann	PROPN
admet-249	120	9	,	,	PUNCT
admet-249	120	10	m.	m.	NOUN
admet-249	120	11	spraul	spraul	PROPN
admet-249	120	12	,	,	PUNCT
admet-249	120	13	h.	h.	PROPN
admet-249	120	14	stuppner	stuppner	PROPN
admet-249	120	15	,	,	PUNCT
admet-249	120	16	f.	f.	PROPN
admet-249	120	17	hadacek	hadacek	PROPN
admet-249	120	18	,	,	PUNCT
admet-249	120	19	journal	journal	NOUN
admet-249	120	20	of	of	ADP
admet-249	120	21	chromatography	chromatography	NOUN
admet-249	120	22	a	a	DET
admet-249	120	23	1136	1136	NUM
admet-249	120	24	(	(	PUNCT
admet-249	120	25	2006	2006	NUM
admet-249	120	26	)	)	PUNCT
admet-249	120	27	82	82	NUM
admet-249	120	28	-	-	SYM
admet-249	120	29	88	88	NUM
admet-249	120	30	.	.	PUNCT
admet-249	121	1	[	[	X
admet-249	121	2	23	23	NUM
admet-249	121	3	]	]	PUNCT
admet-249	121	4	j.	j.	PROPN
admet-249	121	5	larsen	larsen	PROPN
admet-249	121	6	,	,	PUNCT
admet-249	121	7	d.	d.	PROPN
admet-249	121	8	staerk	staerk	PROPN
admet-249	121	9	,	,	PUNCT
admet-249	121	10	c.	c.	PROPN
admet-249	121	11	cornett	cornett	PROPN
admet-249	121	12	,	,	PUNCT
admet-249	121	13	s.	s.	PROPN
admet-249	121	14	h.	h.	PROPN
admet-249	121	15	hansen	hansen	PROPN
admet-249	121	16	,	,	PUNCT
admet-249	121	17	j.	j.	PROPN
admet-249	121	18	w.	w.	PROPN
admet-249	121	19	jaroszewski	jaroszewski	PROPN
admet-249	121	20	,	,	PUNCT
admet-249	121	21	journal	journal	NOUN
admet-249	121	22	of	of	ADP
admet-249	121	23	pharmaceutical	pharmaceutical	NOUN
admet-249	121	24	and	and	CCONJ
admet-249	121	25	biomedical	biomedical	ADJ
admet-249	121	26	anaysis	anaysis	NOUN
admet-249	121	27	49	49	NUM
admet-249	121	28	(	(	PUNCT
admet-249	121	29	2009	2009	NUM
admet-249	121	30	)	)	PUNCT
admet-249	121	31	839–842	839–842	NUM
admet-249	121	32	.	.	PUNCT
admet-249	122	1	©	©	PROPN
admet-249	122	2	2015	2015	NUM
admet-249	122	3	by	by	ADP
admet-249	122	4	the	the	DET
admet-249	122	5	authors	author	NOUN
admet-249	122	6	;	;	PUNCT
admet-249	122	7	licensee	licensee	PROPN
admet-249	122	8	iapc	iapc	PROPN
admet-249	122	9	,	,	PUNCT
admet-249	122	10	zagreb	zagreb	PROPN
admet-249	122	11	,	,	PUNCT
admet-249	122	12	croatia	croatia	PROPN
admet-249	122	13	.	.	PUNCT
admet-249	123	1	this	this	DET
admet-249	123	2	article	article	NOUN
admet-249	123	3	is	be	AUX
admet-249	123	4	an	an	DET
admet-249	123	5	open	open	ADJ
admet-249	123	6	-	-	PUNCT
admet-249	123	7	access	access	NOUN
admet-249	123	8	article	article	NOUN
admet-249	123	9	distributed	distribute	VERB
admet-249	123	10	under	under	ADP
admet-249	123	11	the	the	DET
admet-249	123	12	terms	term	NOUN
admet-249	123	13	and	and	CCONJ
admet-249	123	14	conditions	condition	NOUN
admet-249	123	15	of	of	ADP
admet-249	123	16	the	the	DET
admet-249	123	17	creative	creative	ADJ
admet-249	123	18	commons	common	NOUN
admet-249	123	19	attribution	attribution	NOUN
admet-249	123	20	license	license	NOUN
admet-249	123	21	(	(	PUNCT
admet-249	123	22	http://creativecommons.org/licenses/by/3.0/	http://creativecommons.org/licenses/by/3.0/	PROPN
admet-249	123	23	)	)	PUNCT
admet-249	123	24	http://creativecommons.org/licenses/by/3.0/	http://creativecommons.org/licenses/by/3.0/	PROPN