id	sid	eid	entity	type
american_scientific_journal-3892	1	1	57	CARDINAL
american_scientific_journal-3892	1	2	american scientific research journal	ORG
american_scientific_journal-3892	1	3	issn	PERSON
american_scientific_journal-3892	1	4	2313	CARDINAL
american_scientific_journal-3892	1	5	2313	CARDINAL
american_scientific_journal-3892	1	6	sayadib	GPE
american_scientific_journal-3892	1	7	fathi saftac adoctor	PERSON
american_scientific_journal-3892	1	8	6.5	CARDINAL
american_scientific_journal-3892	1	9	malâa center	ORG
american_scientific_journal-3892	1	10	3042	CARDINAL
american_scientific_journal-3892	1	11	tunisia	GPE
american_scientific_journal-3892	1	12	university of monastir	ORG
american_scientific_journal-3892	1	13	tunisia	GPE
american_scientific_journal-3892	1	14	university of monastir	ORG
american_scientific_journal-3892	1	15	tunisia	GPE
american_scientific_journal-3892	1	16	nine	CARDINAL
american_scientific_journal-3892	3	1	30	CARDINAL
american_scientific_journal-3892	3	2	1.8 μm	QUANTITY
american_scientific_journal-3892	6	1	two	CARDINAL
american_scientific_journal-3892	8	1	seventeen minutes	TIME
american_scientific_journal-3892	8	2	120%	PERCENT
american_scientific_journal-3892	8	3	0.999	CARDINAL
american_scientific_journal-3892	10	1	two	CARDINAL
american_scientific_journal-3892	14	1	american scientific research journal	ORG
american_scientific_journal-3892	14	2	2018	DATE
american_scientific_journal-3892	14	3	41	CARDINAL
american_scientific_journal-3892	14	4	57-75	PERCENT
american_scientific_journal-3892	17	1	1	CARDINAL
american_scientific_journal-3892	18	1	2	CARDINAL
american_scientific_journal-3892	18	2	3	CARDINAL
american_scientific_journal-3892	20	1	3	CARDINAL
american_scientific_journal-3892	21	1	3	CARDINAL
american_scientific_journal-3892	23	1	4	CARDINAL
american_scientific_journal-3892	23	2	5	CARDINAL
american_scientific_journal-3892	24	1	ich q3a	PERSON
american_scientific_journal-3892	24	2	6	CARDINAL
american_scientific_journal-3892	24	3	8	CARDINAL
american_scientific_journal-3892	25	1	daily	DATE
american_scientific_journal-3892	26	1	9	CARDINAL
american_scientific_journal-3892	28	1	four	CARDINAL
american_scientific_journal-3892	28	2	1	CARDINAL
american_scientific_journal-3892	28	3	2	CARDINAL
american_scientific_journal-3892	29	1	3	CARDINAL
american_scientific_journal-3892	30	1	4	CARDINAL
american_scientific_journal-3892	31	1	1	CARDINAL
american_scientific_journal-3892	31	2	2	CARDINAL
american_scientific_journal-3892	31	3	between 50 and 5000 ppm	CARDINAL
american_scientific_journal-3892	31	4	more than 0.5%	PERCENT
american_scientific_journal-3892	32	1	first	ORDINAL
american_scientific_journal-3892	32	2	american	NORP
american_scientific_journal-3892	32	3	2018	DATE
american_scientific_journal-3892	32	4	41	CARDINAL
american_scientific_journal-3892	32	5	57-75 59	CARDINAL
american_scientific_journal-3892	32	6	about 0.1%	PERCENT
american_scientific_journal-3892	32	7	about 1 to 2	CARDINAL
american_scientific_journal-3892	33	1	gc	ORG
american_scientific_journal-3892	34	1	gc	GPE
american_scientific_journal-3892	34	2	10	CARDINAL
american_scientific_journal-3892	34	3	11	CARDINAL
american_scientific_journal-3892	34	4	12	CARDINAL
american_scientific_journal-3892	34	5	13	CARDINAL
american_scientific_journal-3892	36	1	14	CARDINAL
american_scientific_journal-3892	37	1	european	NORP
american_scientific_journal-3892	37	2	chapter 2.4.24 «	LAW
american_scientific_journal-3892	37	3	15	CARDINAL
american_scientific_journal-3892	37	4	two	CARDINAL
american_scientific_journal-3892	40	1	1	CARDINAL
american_scientific_journal-3892	40	2	1	CARDINAL
american_scientific_journal-3892	40	3	2	CARDINAL
american_scientific_journal-3892	40	4	3	CARDINAL
american_scientific_journal-3892	41	1	16	CARDINAL
american_scientific_journal-3892	42	1	17	CARDINAL
american_scientific_journal-3892	44	1	16	CARDINAL
american_scientific_journal-3892	44	2	18	DATE
american_scientific_journal-3892	44	3	19	CARDINAL
american_scientific_journal-3892	45	1	the european pharmacopeia’s	ORG
american_scientific_journal-3892	46	1	16	CARDINAL
american_scientific_journal-3892	46	2	20	CARDINAL
american_scientific_journal-3892	47	1	21	CARDINAL
american_scientific_journal-3892	47	2	22	CARDINAL
american_scientific_journal-3892	48	1	nine	CARDINAL
american_scientific_journal-3892	48	2	2 and 3	DATE
american_scientific_journal-3892	48	3	gc	ORG
american_scientific_journal-3892	48	4	european	NORP
american_scientific_journal-3892	49	1	2	CARDINAL
american_scientific_journal-3892	49	2	2.1	CARDINAL
american_scientific_journal-3892	50	1	china	GPE
american_scientific_journal-3892	50	2	american scientific research journal	ORG
american_scientific_journal-3892	50	3	2018	DATE
american_scientific_journal-3892	50	4	41	CARDINAL
american_scientific_journal-3892	50	5	57-75 60	PERCENT
american_scientific_journal-3892	51	1	2	CARDINAL
american_scientific_journal-3892	51	2	3	CARDINAL
american_scientific_journal-3892	51	3	aldrich	PERSON
american_scientific_journal-3892	51	4	tunisia	GPE
american_scientific_journal-3892	52	1	2.2	CARDINAL
american_scientific_journal-3892	52	2	7694	DATE
american_scientific_journal-3892	53	1	624	CARDINAL
american_scientific_journal-3892	53	2	30	CARDINAL
american_scientific_journal-3892	53	3	0.53 mm	QUANTITY
american_scientific_journal-3892	53	4	1.8 µm	DATE
american_scientific_journal-3892	54	1	table1	ORG
american_scientific_journal-3892	55	1	european	NORP
american_scientific_journal-3892	55	2	about 250 mg	QUANTITY
american_scientific_journal-3892	55	3	25 ml	QUANTITY
american_scientific_journal-3892	55	4	5.0 ml	QUANTITY
american_scientific_journal-3892	55	5	1.0 ml	QUANTITY
american_scientific_journal-3892	56	1	about 500 mg	QUANTITY
american_scientific_journal-3892	56	2	10 ml	QUANTITY
american_scientific_journal-3892	56	3	1.0 ml	QUANTITY
american_scientific_journal-3892	56	4	5.0 ml	QUANTITY
american_scientific_journal-3892	58	1	6%	PERCENT
american_scientific_journal-3892	58	2	cyanopropyl-phenyl(94%	GPE
american_scientific_journal-3892	61	1	30 m×0.32 mm	QUANTITY
american_scientific_journal-3892	61	2	1.8 μm	QUANTITY
american_scientific_journal-3892	61	3	30	CARDINAL
american_scientific_journal-3892	61	4	0.53 mm	QUANTITY
american_scientific_journal-3892	61	5	3.0 μm	QUANTITY
american_scientific_journal-3892	63	1	about 35 cm	QUANTITY
american_scientific_journal-3892	63	2	140°	QUANTITY
american_scientific_journal-3892	64	1	1:5	CARDINAL
american_scientific_journal-3892	64	2	1:3	CARDINAL
american_scientific_journal-3892	65	1	40°	QUANTITY
american_scientific_journal-3892	65	2	20 min	DATE
american_scientific_journal-3892	65	3	240°	QUANTITY
american_scientific_journal-3892	65	4	10°	QUANTITY
american_scientific_journal-3892	65	5	240°	QUANTITY
american_scientific_journal-3892	65	6	20 min	TIME
american_scientific_journal-3892	66	1	250°	QUANTITY
american_scientific_journal-3892	67	1	agilent chemstation	ORG
american_scientific_journal-3892	67	2	3.2.1	CARDINAL
american_scientific_journal-3892	68	1	denver	GPE
american_scientific_journal-3892	69	1	american scientific research journal	ORG
american_scientific_journal-3892	69	2	2018	DATE
american_scientific_journal-3892	69	3	41	CARDINAL
american_scientific_journal-3892	69	4	57-75	PERCENT
american_scientific_journal-3892	70	1	2.3.1	CARDINAL
american_scientific_journal-3892	71	1	european	NORP
american_scientific_journal-3892	71	2	european	NORP
american_scientific_journal-3892	71	3	1	CARDINAL
american_scientific_journal-3892	72	1	15	CARDINAL
american_scientific_journal-3892	73	1	2.3.2	CARDINAL
american_scientific_journal-3892	74	1	gc	ORG
american_scientific_journal-3892	74	2	gc	ORG
american_scientific_journal-3892	74	3	nine	CARDINAL
american_scientific_journal-3892	75	1	the european pharmacopeia	ORG
american_scientific_journal-3892	76	1	2.3.3	CARDINAL
american_scientific_journal-3892	76	2	0.1 g	QUANTITY
american_scientific_journal-3892	76	3	about 0.5	CARDINAL
american_scientific_journal-3892	76	4	20 ml	QUANTITY
american_scientific_journal-3892	76	5	5.0 ml	QUANTITY
american_scientific_journal-3892	77	1	0.2 mg/ml	QUANTITY
american_scientific_journal-3892	77	2	30 ml	QUANTITY
american_scientific_journal-3892	77	3	250 ml	QUANTITY
american_scientific_journal-3892	77	4	about 50 mg	QUANTITY
american_scientific_journal-3892	78	1	30 ml	QUANTITY
american_scientific_journal-3892	78	2	100 ml	QUANTITY
american_scientific_journal-3892	78	3	about 500 mg acetone	QUANTITY
american_scientific_journal-3892	78	4	500	CARDINAL
american_scientific_journal-3892	78	5	500 mg	QUANTITY
american_scientific_journal-3892	78	6	500 mg	QUANTITY
american_scientific_journal-3892	78	7	300 mg methanol	QUANTITY
american_scientific_journal-3892	78	8	60 mg dichloromethane	QUANTITY
american_scientific_journal-3892	78	9	89 mg	QUANTITY
american_scientific_journal-3892	78	10	41 mg	QUANTITY
american_scientific_journal-3892	78	11	72 mg	QUANTITY
american_scientific_journal-3892	79	1	about 0.5 mg/ml	QUANTITY
american_scientific_journal-3892	79	2	0.5 mg	QUANTITY
american_scientific_journal-3892	79	3	0.5 mg/ml	QUANTITY
american_scientific_journal-3892	79	4	0.5 mg/ml	QUANTITY
american_scientific_journal-3892	79	5	0.3 mg/ml	QUANTITY
american_scientific_journal-3892	79	6	0.06 mg/ml	QUANTITY
american_scientific_journal-3892	79	7	0.089 mg/ml	QUANTITY
american_scientific_journal-3892	79	8	0.041 mg/ml	QUANTITY
american_scientific_journal-3892	79	9	0.072 mg/ml	QUANTITY
american_scientific_journal-3892	80	1	the european pharmacopeia	ORG
american_scientific_journal-3892	80	2	5000 ppm	QUANTITY
american_scientific_journal-3892	80	3	5000 ppm	QUANTITY
american_scientific_journal-3892	80	4	5000 ppm	QUANTITY
american_scientific_journal-3892	80	5	5000 ppm	QUANTITY
american_scientific_journal-3892	80	6	3000 ppm	QUANTITY
american_scientific_journal-3892	80	7	methanol	ORG
american_scientific_journal-3892	80	8	600 ppm	QUANTITY
american_scientific_journal-3892	80	9	890 ppm	QUANTITY
american_scientific_journal-3892	80	10	410 ppm	MONEY
american_scientific_journal-3892	80	11	720 ppm	MONEY
american_scientific_journal-3892	80	12	15	CARDINAL
american_scientific_journal-3892	81	1	2.4	CARDINAL
american_scientific_journal-3892	83	1	23-26	CARDINAL
american_scientific_journal-3892	84	1	american	NORP
american_scientific_journal-3892	84	2	2018	DATE
american_scientific_journal-3892	84	3	41	CARDINAL
american_scientific_journal-3892	84	4	57-75 62	PERCENT
american_scientific_journal-3892	84	5	nine	CARDINAL
american_scientific_journal-3892	87	1	120%	PERCENT
american_scientific_journal-3892	87	2	nine	CARDINAL
american_scientific_journal-3892	88	1	120%	PERCENT
american_scientific_journal-3892	88	2	24	CARDINAL
american_scientific_journal-3892	89	1	six	CARDINAL
american_scientific_journal-3892	91	1	120%	PERCENT
american_scientific_journal-3892	91	2	30 ml	QUANTITY
american_scientific_journal-3892	91	3	100 ml	QUANTITY
american_scientific_journal-3892	91	4	600 mg	QUANTITY
american_scientific_journal-3892	91	5	600 mg	QUANTITY
american_scientific_journal-3892	91	6	600 mg	QUANTITY
american_scientific_journal-3892	91	7	600 mg	QUANTITY
american_scientific_journal-3892	91	8	360 mg	QUANTITY
american_scientific_journal-3892	91	9	72 mg	QUANTITY
american_scientific_journal-3892	91	10	106.8 mg	QUANTITY
american_scientific_journal-3892	91	11	49.2 mg	QUANTITY
american_scientific_journal-3892	91	12	86.4 mg	QUANTITY
american_scientific_journal-3892	92	1	1/10	CARDINAL
american_scientific_journal-3892	92	2	2 ml	QUANTITY
american_scientific_journal-3892	92	3	20 ml	QUANTITY
american_scientific_journal-3892	94	1	three	CARDINAL
american_scientific_journal-3892	94	2	120%	PERCENT
american_scientific_journal-3892	94	3	100% and 80%	PERCENT
american_scientific_journal-3892	94	4	0.5	CARDINAL
american_scientific_journal-3892	96	1	two	CARDINAL
american_scientific_journal-3892	97	1	2.4.4	CARDINAL
american_scientific_journal-3892	98	1	three	CARDINAL
american_scientific_journal-3892	100	1	six	CARDINAL
american_scientific_journal-3892	101	1	two	CARDINAL
american_scientific_journal-3892	101	2	days	DATE
american_scientific_journal-3892	102	1	6	CARDINAL
american_scientific_journal-3892	102	2	the same day	DATE
american_scientific_journal-3892	102	3	three consecutive days	DATE
american_scientific_journal-3892	104	1	2.4.5	CARDINAL
american_scientific_journal-3892	105	1	american scientific research journal	ORG
american_scientific_journal-3892	105	2	2018	DATE
american_scientific_journal-3892	105	3	41	CARDINAL
american_scientific_journal-3892	105	4	57-75 63	PERCENT
american_scientific_journal-3892	106	1	loq	ORG
american_scientific_journal-3892	107	1	23	CARDINAL
american_scientific_journal-3892	108	1	lod	ORG
american_scientific_journal-3892	108	2	loq	ORG
american_scientific_journal-3892	108	3	27	CARDINAL
american_scientific_journal-3892	109	1	kumar	PERSON
american_scientific_journal-3892	110	1	27	CARDINAL
american_scientific_journal-3892	111	1	22	CARDINAL
american_scientific_journal-3892	111	2	28	DATE
american_scientific_journal-3892	111	3	29	CARDINAL
american_scientific_journal-3892	112	1	3	CARDINAL
american_scientific_journal-3892	112	2	3.1	CARDINAL
american_scientific_journal-3892	113	1	3.1.1	CARDINAL
american_scientific_journal-3892	114	1	european	NORP
american_scientific_journal-3892	114	2	30 min	TIME
american_scientific_journal-3892	114	3	about 13 min	TIME
american_scientific_journal-3892	115	1	1	CARDINAL
american_scientific_journal-3892	115	2	nine	CARDINAL
american_scientific_journal-3892	116	1	1	CARDINAL
american_scientific_journal-3892	116	2	chromatogram	PERSON
american_scientific_journal-3892	116	3	european	NORP
american_scientific_journal-3892	117	1	bp1	PERSON
american_scientific_journal-3892	117	2	100%	PERCENT
american_scientific_journal-3892	118	1	30	CARDINAL
american_scientific_journal-3892	119	1	27	CARDINAL
american_scientific_journal-3892	120	1	22	CARDINAL
american_scientific_journal-3892	121	1	european	NORP
american_scientific_journal-3892	122	1	2	CARDINAL
american_scientific_journal-3892	123	1	american scientific research journal	ORG
american_scientific_journal-3892	123	2	2018	DATE
american_scientific_journal-3892	123	3	41	CARDINAL
american_scientific_journal-3892	123	4	57-75 64	CARDINAL
american_scientific_journal-3892	124	1	21	CARDINAL
american_scientific_journal-3892	125	1	1,3	CARDINAL
american_scientific_journal-3892	125	2	31	CARDINAL
american_scientific_journal-3892	127	1	21	CARDINAL
american_scientific_journal-3892	128	1	100°	QUANTITY
american_scientific_journal-3892	128	2	32	CARDINAL
american_scientific_journal-3892	130	1	2729	CARDINAL
american_scientific_journal-3892	130	2	32	CARDINAL
american_scientific_journal-3892	131	1	siddiqui	PERSON
american_scientific_journal-3892	131	2	nine	CARDINAL
american_scientific_journal-3892	131	3	22	CARDINAL
american_scientific_journal-3892	132	1	3.1.4	CARDINAL
american_scientific_journal-3892	133	1	3	CARDINAL
american_scientific_journal-3892	134	1	gc	ORG
american_scientific_journal-3892	135	1	four	CARDINAL
american_scientific_journal-3892	135	2	32	CARDINAL
american_scientific_journal-3892	136	1	clécio s	PERSON
american_scientific_journal-3892	136	2	seven	CARDINAL
american_scientific_journal-3892	136	3	28	CARDINAL
american_scientific_journal-3892	137	1	22	CARDINAL
american_scientific_journal-3892	138	1	3.1.5	CARDINAL
american_scientific_journal-3892	138	2	2.1 ml/min	QUANTITY
american_scientific_journal-3892	138	3	35 cm	QUANTITY
american_scientific_journal-3892	138	4	1 ml/min	QUANTITY
american_scientific_journal-3892	138	5	19 cm	QUANTITY
american_scientific_journal-3892	139	1	between 1/5 and 1/1	CARDINAL
american_scientific_journal-3892	140	1	1/1	CARDINAL
american_scientific_journal-3892	141	1	3.1.7	CARDINAL
american_scientific_journal-3892	143	1	2	CARDINAL
american_scientific_journal-3892	143	2	american scientific research journal	ORG
american_scientific_journal-3892	143	3	2018	DATE
american_scientific_journal-3892	143	4	41	CARDINAL
american_scientific_journal-3892	143	5	57-75 65	PERCENT
american_scientific_journal-3892	143	6	40	CARDINAL
american_scientific_journal-3892	144	1	8 min	TIME
american_scientific_journal-3892	144	2	90°	QUANTITY
american_scientific_journal-3892	144	3	10°	QUANTITY
american_scientific_journal-3892	144	4	240°	QUANTITY
american_scientific_journal-3892	144	5	40°	QUANTITY
american_scientific_journal-3892	144	6	5 min	TIME
american_scientific_journal-3892	144	7	2	CARDINAL
american_scientific_journal-3892	144	8	3.2	CARDINAL
american_scientific_journal-3892	145	1	3	CARDINAL
american_scientific_journal-3892	146	1	chromatogram	PERSON
american_scientific_journal-3892	146	2	nine	CARDINAL
american_scientific_journal-3892	147	1	2	CARDINAL
american_scientific_journal-3892	147	2	2	CARDINAL
american_scientific_journal-3892	148	1	kumar.	PERSON
american_scientific_journal-3892	148	2	27	CARDINAL
american_scientific_journal-3892	148	3	30m×0.53 mm	QUANTITY
american_scientific_journal-3892	148	4	1.8 μm	QUANTITY
american_scientific_journal-3892	149	1	45°	QUANTITY
american_scientific_journal-3892	149	2	5 min	TIME
american_scientific_journal-3892	149	3	5°	QUANTITY
american_scientific_journal-3892	149	4	85°	QUANTITY
american_scientific_journal-3892	149	5	12°	QUANTITY
american_scientific_journal-3892	149	6	220°	QUANTITY
american_scientific_journal-3892	149	7	220°	QUANTITY
american_scientific_journal-3892	149	8	260°	QUANTITY
american_scientific_journal-3892	149	9	30m×0.32	CARDINAL
american_scientific_journal-3892	149	10	35°	CARDINAL
american_scientific_journal-3892	149	11	15°	QUANTITY
american_scientific_journal-3892	149	12	40°	QUANTITY
american_scientific_journal-3892	149	13	10 min	TIME
american_scientific_journal-3892	149	14	18°	QUANTITY
american_scientific_journal-3892	149	15	235°	QUANTITY
american_scientific_journal-3892	149	16	8 min	TIME
american_scientific_journal-3892	149	17	35°	QUANTITY
american_scientific_journal-3892	149	18	22	CARDINAL
american_scientific_journal-3892	149	19	100°	QUANTITY
american_scientific_journal-3892	149	20	20 min	TIME
american_scientific_journal-3892	149	21	120°	QUANTITY
american_scientific_journal-3892	149	22	2 min	TIME
american_scientific_journal-3892	149	23	60m×0.250 mm	QUANTITY
american_scientific_journal-3892	149	24	0.25	CARDINAL
american_scientific_journal-3892	150	1	40°	QUANTITY
american_scientific_journal-3892	150	2	5 min	TIME
american_scientific_journal-3892	150	3	10°	QUANTITY
american_scientific_journal-3892	150	4	240°	QUANTITY
american_scientific_journal-3892	150	5	5 min	DATE
american_scientific_journal-3892	150	6	40°	QUANTITY
american_scientific_journal-3892	150	7	250°	QUANTITY
american_scientific_journal-3892	150	8	270°	QUANTITY
american_scientific_journal-3892	151	1	29	CARDINAL
american_scientific_journal-3892	151	2	40°	QUANTITY
american_scientific_journal-3892	151	3	30m×0.53 mm	QUANTITY
american_scientific_journal-3892	151	4	3.0 μm	QUANTITY
american_scientific_journal-3892	152	1	40°	QUANTITY
american_scientific_journal-3892	152	2	6 min	QUANTITY
american_scientific_journal-3892	152	3	10°	QUANTITY
american_scientific_journal-3892	152	4	130°	QUANTITY
american_scientific_journal-3892	152	5	8 min	TIME
american_scientific_journal-3892	152	6	35°	QUANTITY
american_scientific_journal-3892	152	7	240°	QUANTITY
american_scientific_journal-3892	152	8	5 min 100°	QUANTITY
american_scientific_journal-3892	152	9	250°	QUANTITY
american_scientific_journal-3892	152	10	c.m.	GPE
american_scientific_journal-3892	152	11	32	CARDINAL
american_scientific_journal-3892	152	12	105°	QUANTITY
american_scientific_journal-3892	152	13	45 min	QUANTITY
american_scientific_journal-3892	152	14	2.5 ml	QUANTITY
american_scientific_journal-3892	152	15	624	CARDINAL
american_scientific_journal-3892	152	16	30m×0.53 mm	QUANTITY
american_scientific_journal-3892	152	17	3.00	CARDINAL
american_scientific_journal-3892	153	1	40°	QUANTITY
american_scientific_journal-3892	153	2	20 min	TIME
american_scientific_journal-3892	153	3	10°	QUANTITY
american_scientific_journal-3892	153	4	240°	QUANTITY
american_scientific_journal-3892	153	5	20 min fid	QUANTITY
american_scientific_journal-3892	153	6	american scientific research journal	ORG
american_scientific_journal-3892	153	7	2018	DATE
american_scientific_journal-3892	153	8	41	CARDINAL
american_scientific_journal-3892	153	9	57-75 66	CARDINAL
american_scientific_journal-3892	153	10	3	CARDINAL
american_scientific_journal-3892	153	11	6%	PERCENT
american_scientific_journal-3892	153	12	polycyanopropyl-phenyl-siloxane	PERSON
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american_scientific_journal-3892	154	1	30	CARDINAL
american_scientific_journal-3892	154	2	0.53 mm	QUANTITY
american_scientific_journal-3892	154	3	1.8 μm	QUANTITY
american_scientific_journal-3892	155	1	1 ml/min	QUANTITY
american_scientific_journal-3892	155	2	1:1	CARDINAL
american_scientific_journal-3892	155	3	40°	QUANTITY
american_scientific_journal-3892	155	4	8 min	TIME
american_scientific_journal-3892	155	5	90°	QUANTITY
american_scientific_journal-3892	155	6	10°	QUANTITY
american_scientific_journal-3892	155	7	240°	QUANTITY
american_scientific_journal-3892	155	8	40°	QUANTITY
american_scientific_journal-3892	156	1	140°	QUANTITY
american_scientific_journal-3892	156	2	250°	QUANTITY
american_scientific_journal-3892	156	3	2	CARDINAL
american_scientific_journal-3892	156	4	chromatogram	PERSON
american_scientific_journal-3892	156	5	nine	CARDINAL
american_scientific_journal-3892	157	1	3.3	CARDINAL
american_scientific_journal-3892	158	1	3.3.1	CARDINAL
american_scientific_journal-3892	159	1	3	CARDINAL
american_scientific_journal-3892	159	2	2	CARDINAL
american_scientific_journal-3892	159	3	4	CARDINAL
american_scientific_journal-3892	160	1	3.3.2	CARDINAL
american_scientific_journal-3892	160	2	29	CARDINAL
american_scientific_journal-3892	160	3	32	DATE
american_scientific_journal-3892	162	1	american scientific research journal	ORG
american_scientific_journal-3892	162	2	2018	DATE
american_scientific_journal-3892	162	3	41	CARDINAL
american_scientific_journal-3892	162	4	57-75 67	PERCENT
american_scientific_journal-3892	162	5	3	CARDINAL
american_scientific_journal-3892	162	6	chromatogram	PERSON
american_scientific_journal-3892	163	1	4	CARDINAL
american_scientific_journal-3892	163	2	4.28 0.27	CARDINAL
american_scientific_journal-3892	163	3	5.70	CARDINAL
american_scientific_journal-3892	163	4	6.67 0.43	CARDINAL
american_scientific_journal-3892	163	5	7.03	CARDINAL
american_scientific_journal-3892	163	6	7.05 0.45 2.69	CARDINAL
american_scientific_journal-3892	163	7	7.41 0.47 2.44	QUANTITY
american_scientific_journal-3892	163	8	7.91 0.51 3.52 ethyl	QUANTITY
american_scientific_journal-3892	163	9	11.27 0.72 27.5	QUANTITY
american_scientific_journal-3892	163	10	11.67	CARDINAL
american_scientific_journal-3892	163	11	15.04	CARDINAL
american_scientific_journal-3892	163	12	47.64	CARDINAL
american_scientific_journal-3892	163	13	15.61 1.00	CARDINAL
american_scientific_journal-3892	163	14	16.00	CARDINAL
american_scientific_journal-3892	163	15	1.02 12.85	CARDINAL
american_scientific_journal-3892	163	16	5	CARDINAL
american_scientific_journal-3892	163	17	r2 linear	GPE
american_scientific_journal-3892	163	18	r2 methanol	ORG
american_scientific_journal-3892	164	1	0.999	CARDINAL
american_scientific_journal-3892	164	2	0.999	CARDINAL
american_scientific_journal-3892	164	3	0.999	CARDINAL
american_scientific_journal-3892	164	4	0.0661x-9.6613	CARDINAL
american_scientific_journal-3892	165	1	y=0.0861x-0.2571	GPE
american_scientific_journal-3892	165	2	0.9904	CARDINAL
american_scientific_journal-3892	165	3	y=0.0529x-0.0306	GPE
american_scientific_journal-3892	165	4	0.9992 ethyl	QUANTITY
american_scientific_journal-3892	165	5	0.9998	CARDINAL
american_scientific_journal-3892	165	6	0.9598	CARDINAL
american_scientific_journal-3892	166	1	0.9998 toluene	QUANTITY
american_scientific_journal-3892	166	2	0.9995	CARDINAL
american_scientific_journal-3892	166	3	2018	DATE
american_scientific_journal-3892	166	4	41	CARDINAL
american_scientific_journal-3892	166	5	57-75 68	PERCENT
american_scientific_journal-3892	166	6	120%	PERCENT
american_scientific_journal-3892	166	7	0.999	CARDINAL
american_scientific_journal-3892	167	1	5	CARDINAL
american_scientific_journal-3892	169	1	loq	ORG
american_scientific_journal-3892	169	2	1	CARDINAL
american_scientific_journal-3892	169	3	2	CARDINAL
american_scientific_journal-3892	170	1	3.3	CARDINAL
american_scientific_journal-3892	170	2	1	CARDINAL
american_scientific_journal-3892	170	3	10	CARDINAL
american_scientific_journal-3892	170	4	2	CARDINAL
american_scientific_journal-3892	170	5	6	CARDINAL
american_scientific_journal-3892	173	1	9	CARDINAL
american_scientific_journal-3892	174	1	6	CARDINAL
american_scientific_journal-3892	174	2	76.65	CARDINAL
american_scientific_journal-3892	174	3	232.28	CARDINAL
american_scientific_journal-3892	174	4	83.97	CARDINAL
american_scientific_journal-3892	174	5	118.09	MONEY
american_scientific_journal-3892	174	6	59.97	CARDINAL
american_scientific_journal-3892	174	7	181.73	CARDINAL
american_scientific_journal-3892	174	8	83.59	CARDINAL
american_scientific_journal-3892	174	9	9.41 28.52	CARDINAL
american_scientific_journal-3892	174	10	65.08	CARDINAL
american_scientific_journal-3892	174	11	197.22	MONEY
american_scientific_journal-3892	174	12	14.36	CARDINAL
american_scientific_journal-3892	174	13	43.52	MONEY
american_scientific_journal-3892	174	14	19.38	CARDINAL
american_scientific_journal-3892	175	1	intra-day	DATE
american_scientific_journal-3892	175	2	less than 5.0%	PERCENT
american_scientific_journal-3892	175	3	7	CARDINAL
american_scientific_journal-3892	176	1	6%	PERCENT
american_scientific_journal-3892	176	2	less than 6%	PERCENT
american_scientific_journal-3892	177	1	american scientific research journal	ORG
american_scientific_journal-3892	177	2	2018	DATE
american_scientific_journal-3892	177	3	41	CARDINAL
american_scientific_journal-3892	177	4	57-75 69	PERCENT
american_scientific_journal-3892	177	5	one	CARDINAL
american_scientific_journal-3892	178	1	7	CARDINAL
american_scientific_journal-3892	178	2	the internal standard methanol	ORG
american_scientific_journal-3892	178	3	2.81	CARDINAL
american_scientific_journal-3892	178	4	3.12	CARDINAL
american_scientific_journal-3892	178	5	1.93 1.56	QUANTITY
american_scientific_journal-3892	178	6	1.31 1.15	CARDINAL
american_scientific_journal-3892	178	7	1.5 0.47	QUANTITY
american_scientific_journal-3892	178	8	3.53	CARDINAL
american_scientific_journal-3892	178	9	1.00 2.12 ethyl	QUANTITY
american_scientific_journal-3892	178	10	3.66 3.52	CARDINAL
american_scientific_journal-3892	178	11	1.26 0.79	QUANTITY
american_scientific_journal-3892	178	12	1.47 0.29	CARDINAL
american_scientific_journal-3892	178	13	8	CARDINAL
american_scientific_journal-3892	179	1	±	CARDINAL
american_scientific_journal-3892	179	2	±	CARDINAL
american_scientific_journal-3892	179	3	120%	PERCENT
american_scientific_journal-3892	179	4	88.37 ± 7.85	MONEY
american_scientific_journal-3892	179	5	98.25	MONEY
american_scientific_journal-3892	179	6	99.12 100%	PERCENT
american_scientific_journal-3892	179	7	102.12 ±	MONEY
american_scientific_journal-3892	179	8	100.02	CARDINAL
american_scientific_journal-3892	179	9	106.60	CARDINAL
american_scientific_journal-3892	179	10	101.02 80%	PERCENT
american_scientific_journal-3892	179	11	2.84	MONEY
american_scientific_journal-3892	179	12	104.10	MONEY
american_scientific_journal-3892	179	13	3.3.5	PRODUCT
american_scientific_journal-3892	180	1	3	CARDINAL
american_scientific_journal-3892	181	1	recovery %	PERCENT
american_scientific_journal-3892	181	2	80%	PERCENT
american_scientific_journal-3892	181	3	100%	PERCENT
american_scientific_journal-3892	181	4	120%	PERCENT
american_scientific_journal-3892	181	5	𝐴𝐴𝐴𝐴𝐴𝐴𝐴𝐴	PERSON
american_scientific_journal-3892	181	6	𝑠𝑠𝑝𝑝𝑠𝑠𝑝𝑝𝐴𝐴𝑠𝑠	GPE
american_scientific_journal-3892	181	7	𝐴𝐴𝐴𝐴𝐴𝐴𝐴𝐴	PERSON
american_scientific_journal-3892	181	8	𝑠𝑠𝑝𝑝𝑠𝑠𝑝𝑝𝐴𝐴𝑠𝑠	GPE
american_scientific_journal-3892	181	9	𝐴𝐴𝐴𝐴𝐴𝐴𝐴𝐴𝐴𝐴𝐴𝐴𝐴𝐴	GPE
american_scientific_journal-3892	181	10	𝐴𝐴𝐴𝐴𝐴𝐴𝐴𝐴	PERSON
american_scientific_journal-3892	181	11	𝑠𝑠𝑜𝑜𝑠𝑠𝑠𝑠𝑠𝑠𝑠𝑠𝑜𝑜𝑠𝑠 × 100	PRODUCT
american_scientific_journal-3892	181	12	3	CARDINAL
american_scientific_journal-3892	181	13	american scientific research journal	ORG
american_scientific_journal-3892	181	14	2018	DATE
american_scientific_journal-3892	181	15	41	CARDINAL
american_scientific_journal-3892	181	16	57-75 70	MONEY
american_scientific_journal-3892	181	17	two	CARDINAL
american_scientific_journal-3892	182	1	mean± s.d.	LOC
american_scientific_journal-3892	183	1	9	CARDINAL
american_scientific_journal-3892	183	2	between 85% and 115%	PERCENT
american_scientific_journal-3892	184	1	9	CARDINAL
american_scientific_journal-3892	184	2	j2 j3 j1 j2 j3 methanol	ORG
american_scientific_journal-3892	184	3	2.13	CARDINAL
american_scientific_journal-3892	184	4	1.11 5.28	CARDINAL
american_scientific_journal-3892	184	5	1.59	CARDINAL
american_scientific_journal-3892	184	6	1.93 2.02 5.17	QUANTITY
american_scientific_journal-3892	184	7	0.94	CARDINAL
american_scientific_journal-3892	184	8	4.04	CARDINAL
american_scientific_journal-3892	184	9	3.08	CARDINAL
american_scientific_journal-3892	184	10	1.35 4.92	QUANTITY
american_scientific_journal-3892	184	11	1.12 1.00	CARDINAL
american_scientific_journal-3892	184	12	1.33	CARDINAL
american_scientific_journal-3892	184	13	3.52 1.10 3.34	QUANTITY
american_scientific_journal-3892	184	14	1.89 1.26 1.24 17.00 1.89 1.26 1.24 5.44	MONEY
american_scientific_journal-3892	184	15	1.61 1.47 0.79	QUANTITY
american_scientific_journal-3892	184	16	5.50	CARDINAL
american_scientific_journal-3892	184	17	10	CARDINAL
american_scientific_journal-3892	184	18	±	CARDINAL
american_scientific_journal-3892	185	1	±	CARDINAL
american_scientific_journal-3892	185	2	120%	PERCENT
american_scientific_journal-3892	185	3	97.04	CARDINAL
american_scientific_journal-3892	185	4	92.59	CARDINAL
american_scientific_journal-3892	185	5	100%	PERCENT
american_scientific_journal-3892	185	6	106.11	CARDINAL
american_scientific_journal-3892	185	7	111.00 97.49	CARDINAL
american_scientific_journal-3892	185	8	97.83 80%	PERCENT
american_scientific_journal-3892	185	9	111.48	CARDINAL
american_scientific_journal-3892	185	10	101.28	CARDINAL
american_scientific_journal-3892	185	11	107.36	CARDINAL
american_scientific_journal-3892	185	12	90%	PERCENT
american_scientific_journal-3892	185	13	110%	PERCENT
american_scientific_journal-3892	185	14	80%	PERCENT
american_scientific_journal-3892	185	15	27	CARDINAL
american_scientific_journal-3892	185	16	29	CARDINAL
american_scientific_journal-3892	186	1	28	CARDINAL
american_scientific_journal-3892	186	2	29	CARDINAL
american_scientific_journal-3892	188	1	american scientific research journal	ORG
american_scientific_journal-3892	188	2	2018	DATE
american_scientific_journal-3892	188	3	41	CARDINAL
american_scientific_journal-3892	188	4	57-75	PERCENT
american_scientific_journal-3892	191	1	chromatogram	PERSON
american_scientific_journal-3892	192	1	chromatogram	PERSON
american_scientific_journal-3892	192	2	loq	ORG
american_scientific_journal-3892	192	3	4	CARDINAL
american_scientific_journal-3892	193	1	4	CARDINAL
american_scientific_journal-3892	193	2	ae	ORG
american_scientific_journal-3892	193	3	astd	ORG
american_scientific_journal-3892	194	1	42.35 ppm	MONEY
american_scientific_journal-3892	194	2	41.92 ppm	MONEY
american_scientific_journal-3892	194	3	3000 ppm	MONEY
american_scientific_journal-3892	195	1	4	CARDINAL
american_scientific_journal-3892	198	1	the european pharmacopeia	ORG
american_scientific_journal-3892	198	2	3	CARDINAL
american_scientific_journal-3892	199	1	nine	CARDINAL
american_scientific_journal-3892	199	2	2 and 3	DATE
american_scientific_journal-3892	200	1	european	NORP
american_scientific_journal-3892	201	1	chromatogram	PERSON
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american_scientific_journal-3892	201	3	2018	DATE
american_scientific_journal-3892	201	4	41	CARDINAL
american_scientific_journal-3892	201	5	57-75 72	PERCENT
american_scientific_journal-3892	201	6	seventeen minutes	TIME
american_scientific_journal-3892	202	1	5%	PERCENT
american_scientific_journal-3892	202	2	6%	PERCENT
american_scientific_journal-3892	202	3	linear	ORG
american_scientific_journal-3892	202	4	120%	PERCENT
american_scientific_journal-3892	202	5	0.999	CARDINAL
american_scientific_journal-3892	204	1	two	CARDINAL
american_scientific_journal-3892	207	1	5	CARDINAL
american_scientific_journal-3892	207	2	gc	ORG
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american_scientific_journal-3892	210	1	° 2011/8	DATE
american_scientific_journal-3892	211	1	2	CARDINAL
american_scientific_journal-3892	213	1	eur j pharm biopharm	ORG
american_scientific_journal-3892	214	1	43	DATE
american_scientific_journal-3892	215	1	215-42	CARDINAL
american_scientific_journal-3892	216	1	3	CARDINAL
american_scientific_journal-3892	216	2	a. ghassempour	PERSON
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american_scientific_journal-3892	220	1	983-88	CARDINAL
american_scientific_journal-3892	221	1	4	CARDINAL
american_scientific_journal-3892	221	2	berridge	PERSON
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american_scientific_journal-3892	224	1	5	CARDINAL
american_scientific_journal-3892	224	2	md.	GPE
american_scientific_journal-3892	224	3	argentine	NORP
american_scientific_journal-3892	224	4	owens	PERSON
american_scientific_journal-3892	224	5	olsen	PERSON
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american_scientific_journal-3892	226	2	28, 2007	DATE
american_scientific_journal-3892	227	1	6	CARDINAL
american_scientific_journal-3892	227	2	d’impuretés dans les nouvelles	PERSON
american_scientific_journal-3892	227	3	thème q3a	PERSON
american_scientific_journal-3892	228	1	2003 septembre 25	DATE
american_scientific_journal-3892	229	1	https://www.ncbi.nlm.nih.gov/pubmed/?term=darbandi%20mk%5bauthor%5d&cauthor=true&cauthor_uid=15620523 https://www.ncbi.nlm.nih.gov/pubmed/?term=ahmadi%20sh%5bauthor%5d&cauthor=true&cauthor_uid=15620523 http://europepmc.org/search;jsessionid=dc87f7bb59dc6e6003f0a483e1a54d93?query=auth:%22owens+pk%22&page=1 american	PERSON
american_scientific_journal-3892	229	2	2018	DATE
american_scientific_journal-3892	229	3	41	CARDINAL
american_scientific_journal-3892	229	4	57-75 73	MONEY
american_scientific_journal-3892	230	1	7	CARDINAL
american_scientific_journal-3892	232	1	2006	DATE
american_scientific_journal-3892	233	1	2__guideline.pdf/	CARDINAL
american_scientific_journal-3892	233	2	8	CARDINAL
american_scientific_journal-3892	235	1	2006	DATE
american_scientific_journal-3892	235	2	2	CARDINAL
american_scientific_journal-3892	236	1	9	CARDINAL
american_scientific_journal-3892	239	1	2011	DATE
american_scientific_journal-3892	240	1	10	CARDINAL
american_scientific_journal-3892	241	1	haky	ORG
american_scientific_journal-3892	241	2	stickney	ORG
american_scientific_journal-3892	243	1	j. chromatogr	PERSON
american_scientific_journal-3892	243	2	1985	DATE
american_scientific_journal-3892	244	1	11	CARDINAL
american_scientific_journal-3892	246	1	pp.1327–31	GPE
american_scientific_journal-3892	246	2	1991	DATE
american_scientific_journal-3892	247	1	12	CARDINAL
american_scientific_journal-3892	247	2	f. ruchatz	PERSON
american_scientific_journal-3892	250	1	j. pharm	ORG
american_scientific_journal-3892	250	2	73, 1996	DATE
american_scientific_journal-3892	251	1	13	CARDINAL
american_scientific_journal-3892	251	2	markovich	PERSON
american_scientific_journal-3892	251	3	s. ong	PERSON
american_scientific_journal-3892	251	4	j. rosen	PERSON
american_scientific_journal-3892	253	1	j. chromatogr	PERSON
american_scientific_journal-3892	254	1	sci	ORG
american_scientific_journal-3892	255	1	14	CARDINAL
american_scientific_journal-3892	258	1	curr	PERSON
american_scientific_journal-3892	259	1	pp.79-83, 2005	DATE
american_scientific_journal-3892	260	1	15	CARDINAL
american_scientific_journal-3892	260	2	2.4.24	CARDINAL
american_scientific_journal-3892	260	3	european	NORP
american_scientific_journal-3892	260	4	8th ed	LOC
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american_scientific_journal-3892	260	6	2014	DATE
american_scientific_journal-3892	261	1	16	CARDINAL
american_scientific_journal-3892	261	2	balarm	GPE
american_scientific_journal-3892	263	1	trac	PERSON
american_scientific_journal-3892	263	2	pp.83-95	DATE
american_scientific_journal-3892	263	3	2016	DATE
american_scientific_journal-3892	264	1	american scientific research journal	ORG
american_scientific_journal-3892	264	2	2018	DATE
american_scientific_journal-3892	264	3	41	CARDINAL
american_scientific_journal-3892	264	4	57-75 74	MONEY
american_scientific_journal-3892	265	1	17	CARDINAL
american_scientific_journal-3892	265	2	lee	PERSON
american_scientific_journal-3892	265	3	c. nguyen van dau	PERSON
american_scientific_journal-3892	266	1	krastulović	PERSON
american_scientific_journal-3892	267	1	european	NORP
american_scientific_journal-3892	268	1	international journal of pharmaceutics	ORG
american_scientific_journal-3892	268	2	1-2	CARDINAL
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american_scientific_journal-3892	269	1	18	CARDINAL
american_scientific_journal-3892	270	1	poole	GPE
american_scientific_journal-3892	272	1	amsterdam	GPE
american_scientific_journal-3892	272	2	2003	DATE
american_scientific_journal-3892	273	1	19	CARDINAL
american_scientific_journal-3892	273	2	mcnair	PERSON
american_scientific_journal-3892	273	3	jm	ORG
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american_scientific_journal-3892	274	1	2nd	ORDINAL
american_scientific_journal-3892	274	2	2009	DATE
american_scientific_journal-3892	275	1	20	CARDINAL
american_scientific_journal-3892	275	2	n. jacek	PERSON
american_scientific_journal-3892	275	3	s. wiesław	PERSON
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