id	sid	tid	token	lemma	pos
cet-3413	1	1	microsoft	microsoft	PROPN
cet-3413	1	2	word	word	PROPN
cet-3413	1	3	025.docx	025.docx	PROPN
cet-3413	1	4	chemical	chemical	NOUN
cet-3413	1	5	engineering	engineering	NOUN
cet-3413	1	6	transactions	transaction	NOUN
cet-3413	1	7	vol	vol	NOUN
cet-3413	1	8	.	.	PUNCT
cet-3413	2	1	48	48	NUM
cet-3413	2	2	,	,	PUNCT
cet-3413	2	3	2016	2016	NUM
cet-3413	2	4	a	a	DET
cet-3413	2	5	publication	publication	NOUN
cet-3413	2	6	of	of	ADP
cet-3413	2	7	the	the	DET
cet-3413	2	8	italian	italian	ADJ
cet-3413	2	9	association	association	NOUN
cet-3413	2	10	of	of	ADP
cet-3413	2	11	chemical	chemical	PROPN
cet-3413	2	12	engineering	engineering	NOUN
cet-3413	2	13	online	online	ADV
cet-3413	2	14	at	at	ADP
cet-3413	2	15	www.aidic.it/cet	www.aidic.it/cet	PROPN
cet-3413	2	16	guest	guest	NOUN
cet-3413	2	17	editors	editor	NOUN
cet-3413	2	18	:	:	PUNCT
cet-3413	2	19	eddy	eddy	PROPN
cet-3413	2	20	de	de	PROPN
cet-3413	2	21	rademaeker	rademaeker	PROPN
cet-3413	2	22	,	,	PUNCT
cet-3413	2	23	peter	peter	PROPN
cet-3413	2	24	schmelzer	schmelzer	PROPN
cet-3413	2	25	copyright	copyright	NOUN
cet-3413	2	26	©	©	PROPN
cet-3413	2	27	2016	2016	NUM
cet-3413	2	28	,	,	PUNCT
cet-3413	2	29	aidic	aidic	ADJ
cet-3413	2	30	servizi	servizi	PROPN
cet-3413	2	31	s.r.l	s.r.l	NOUN
cet-3413	2	32	.	.	PUNCT
cet-3413	2	33	,	,	PUNCT
cet-3413	2	34	isbn	isbn	PROPN
cet-3413	2	35	978	978	NUM
cet-3413	2	36	-	-	SYM
cet-3413	2	37	88	88	NUM
cet-3413	2	38	-	-	PUNCT
cet-3413	2	39	95608	95608	NUM
cet-3413	2	40	-	-	PUNCT
cet-3413	2	41	39	39	NUM
cet-3413	2	42	-	-	SYM
cet-3413	2	43	6	6	NUM
cet-3413	2	44	;	;	PUNCT
cet-3413	2	45	issn	issn	PROPN
cet-3413	2	46	2283	2283	NUM
cet-3413	2	47	-	-	SYM
cet-3413	2	48	9216	9216	NUM
cet-3413	2	49	thermal	thermal	ADJ
cet-3413	2	50	stability	stability	NOUN
cet-3413	2	51	of	of	ADP
cet-3413	2	52	amine	amine	ADJ
cet-3413	2	53	compounds	compound	NOUN
cet-3413	2	54	and	and	CCONJ
cet-3413	2	55	dichloromethane	dichloromethane	NOUN
cet-3413	2	56	carlota	carlota	PROPN
cet-3413	2	57	hernandez*a	hernandez*a	PROPN
cet-3413	2	58	,	,	PUNCT
cet-3413	2	59	stephan	stephan	PROPN
cet-3413	2	60	dreischa	dreischa	PROPN
cet-3413	2	61	,	,	PUNCT
cet-3413	2	62	jörg	jörg	PROPN
cet-3413	2	63	horna	horna	PROPN
cet-3413	2	64	,	,	PUNCT
cet-3413	2	65	steffen	steffen	PROPN
cet-3413	2	66	neuenfeldb	neuenfeldb	PROPN
cet-3413	2	67	aconsilab	aconsilab	PROPN
cet-3413	2	68	gesellschaft	gesellschaft	PROPN
cet-3413	2	69	für	für	PROPN
cet-3413	2	70	anlagensicherheit	anlagensicherheit	PROPN
cet-3413	2	71	mbh	mbh	PROPN
cet-3413	2	72	,	,	PUNCT
cet-3413	2	73	industriepark	industriepark	NOUN
cet-3413	2	74	höchst	höchst	NOUN
cet-3413	2	75	,	,	PUNCT
cet-3413	2	76	65926	65926	NUM
cet-3413	2	77	frankfurt	frankfurt	PROPN
cet-3413	2	78	am	be	AUX
cet-3413	2	79	main	main	ADJ
cet-3413	2	80	,	,	PUNCT
cet-3413	2	81	germany	germany	PROPN
cet-3413	2	82	bmerck	bmerck	PROPN
cet-3413	2	83	kgaa	kgaa	PROPN
cet-3413	2	84	,	,	PUNCT
cet-3413	2	85	frankfurter	frankfurter	PROPN
cet-3413	2	86	str	str	PROPN
cet-3413	2	87	.	.	PROPN
cet-3413	3	1	250	250	NUM
cet-3413	3	2	,	,	PUNCT
cet-3413	3	3	64293	64293	NUM
cet-3413	3	4	darmstadt	darmstadt	PROPN
cet-3413	3	5	,	,	PUNCT
cet-3413	3	6	germany	germany	PROPN
cet-3413	3	7	carlota.hernandez.guri@consilab.de	carlota.hernandez.guri@consilab.de	PROPN
cet-3413	3	8	dichloromethane	dichloromethane	NOUN
cet-3413	3	9	is	be	AUX
cet-3413	3	10	employed	employ	VERB
cet-3413	3	11	as	as	ADP
cet-3413	3	12	a	a	DET
cet-3413	3	13	common	common	ADJ
cet-3413	3	14	solvent	solvent	NOUN
cet-3413	3	15	in	in	ADP
cet-3413	3	16	the	the	DET
cet-3413	3	17	chemical	chemical	NOUN
cet-3413	3	18	industry	industry	NOUN
cet-3413	3	19	.	.	PUNCT
cet-3413	4	1	due	due	ADP
cet-3413	4	2	to	to	ADP
cet-3413	4	3	its	its	PRON
cet-3413	4	4	low	low	ADJ
cet-3413	4	5	boiling	boiling	NOUN
cet-3413	4	6	point	point	NOUN
cet-3413	4	7	of	of	ADP
cet-3413	4	8	39.7	39.7	NUM
cet-3413	4	9	°	°	NOUN
cet-3413	4	10	c	c	NOUN
cet-3413	4	11	it	it	PRON
cet-3413	4	12	can	can	AUX
cet-3413	4	13	be	be	AUX
cet-3413	4	14	used	use	VERB
cet-3413	4	15	for	for	ADP
cet-3413	4	16	the	the	DET
cet-3413	4	17	extraction	extraction	NOUN
cet-3413	4	18	of	of	ADP
cet-3413	4	19	amine	amine	ADJ
cet-3413	4	20	compounds	compound	NOUN
cet-3413	4	21	.	.	PUNCT
cet-3413	5	1	however	however	ADV
cet-3413	5	2	,	,	PUNCT
cet-3413	5	3	caution	caution	NOUN
cet-3413	5	4	is	be	AUX
cet-3413	5	5	advised	advise	VERB
cet-3413	5	6	while	while	SCONJ
cet-3413	5	7	handling	handle	VERB
cet-3413	5	8	and	and	CCONJ
cet-3413	5	9	storing	store	VERB
cet-3413	5	10	amine	amine	ADJ
cet-3413	5	11	compounds	compound	NOUN
cet-3413	5	12	diluted	dilute	VERB
cet-3413	5	13	in	in	ADP
cet-3413	5	14	dichloromethane	dichloromethane	NOUN
cet-3413	5	15	,	,	PUNCT
cet-3413	5	16	since	since	SCONJ
cet-3413	5	17	there	there	PRON
cet-3413	5	18	were	be	VERB
cet-3413	5	19	incidents	incident	NOUN
cet-3413	5	20	with	with	ADP
cet-3413	5	21	unexpected	unexpected	ADJ
cet-3413	5	22	reactions	reaction	NOUN
cet-3413	5	23	between	between	ADP
cet-3413	5	24	amine	amine	ADJ
cet-3413	5	25	compounds	compound	NOUN
cet-3413	5	26	and	and	CCONJ
cet-3413	5	27	dichloromethane	dichloromethane	NOUN
cet-3413	5	28	in	in	ADP
cet-3413	5	29	the	the	DET
cet-3413	5	30	past	past	NOUN
cet-3413	5	31	(	(	PUNCT
cet-3413	5	32	bretherick	bretherick	PROPN
cet-3413	5	33	’s	’s	PART
cet-3413	5	34	handbook	handbook	NOUN
cet-3413	5	35	of	of	ADP
cet-3413	5	36	reactive	reactive	ADJ
cet-3413	5	37	chemical	chemical	NOUN
cet-3413	5	38	hazards	hazard	NOUN
cet-3413	5	39	,	,	PUNCT
cet-3413	5	40	2007	2007	NUM
cet-3413	5	41	)	)	PUNCT
cet-3413	5	42	.	.	PUNCT
cet-3413	6	1	for	for	ADP
cet-3413	6	2	instance	instance	NOUN
cet-3413	6	3	,	,	PUNCT
cet-3413	6	4	an	an	DET
cet-3413	6	5	exothermic	exothermic	ADJ
cet-3413	6	6	reaction	reaction	NOUN
cet-3413	6	7	occurred	occur	VERB
cet-3413	6	8	during	during	ADP
cet-3413	6	9	a	a	DET
cet-3413	6	10	distillation	distillation	NOUN
cet-3413	6	11	at	at	ADP
cet-3413	6	12	30	30	NUM
cet-3413	6	13	°	°	NOUN
cet-3413	6	14	c	c	NOUN
cet-3413	6	15	of	of	ADP
cet-3413	6	16	a	a	DET
cet-3413	6	17	mixture	mixture	NOUN
cet-3413	6	18	of	of	ADP
cet-3413	6	19	ethylene	ethylene	NOUN
cet-3413	6	20	diamine	diamine	NOUN
cet-3413	6	21	and	and	CCONJ
cet-3413	6	22	dichloromethane	dichloromethane	NOUN
cet-3413	6	23	,	,	PUNCT
cet-3413	6	24	which	which	PRON
cet-3413	6	25	subsequently	subsequently	ADV
cet-3413	6	26	deflagrated	deflagrate	VERB
cet-3413	6	27	(	(	PUNCT
cet-3413	6	28	nolan	nolan	PROPN
cet-3413	6	29	,	,	PUNCT
cet-3413	6	30	1983	1983	NUM
cet-3413	6	31	)	)	PUNCT
cet-3413	6	32	.	.	PUNCT
cet-3413	7	1	in	in	ADP
cet-3413	7	2	a	a	DET
cet-3413	7	3	later	later	ADJ
cet-3413	7	4	study	study	NOUN
cet-3413	7	5	,	,	PUNCT
cet-3413	7	6	the	the	DET
cet-3413	7	7	decomposition	decomposition	NOUN
cet-3413	7	8	energy	energy	NOUN
cet-3413	7	9	was	be	AUX
cet-3413	7	10	determined	determine	VERB
cet-3413	7	11	as	as	ADP
cet-3413	7	12	∆hr	∆hr	X
cet-3413	8	1	=	=	NOUN
cet-3413	8	2	-343	-343	PROPN
cet-3413	8	3	kj	kj	PROPN
cet-3413	8	4	/	/	SYM
cet-3413	8	5	mol	mol	PROPN
cet-3413	8	6	(	(	PUNCT
cet-3413	8	7	4.04	4.04	NUM
cet-3413	8	8	kj	kj	PROPN
cet-3413	8	9	/	/	SYM
cet-3413	8	10	g	g	NOUN
cet-3413	8	11	)	)	PUNCT
cet-3413	8	12	based	base	VERB
cet-3413	8	13	on	on	ADP
cet-3413	8	14	the	the	DET
cet-3413	8	15	amount	amount	NOUN
cet-3413	8	16	of	of	ADP
cet-3413	8	17	dichloromethane	dichloromethane	NOUN
cet-3413	8	18	(	(	PUNCT
cet-3413	8	19	heskey	heskey	NOUN
cet-3413	8	20	,	,	PUNCT
cet-3413	8	21	1986	1986	NUM
cet-3413	8	22	)	)	PUNCT
cet-3413	8	23	.	.	PUNCT
cet-3413	9	1	further	further	ADJ
cet-3413	9	2	incidents	incident	NOUN
cet-3413	9	3	in	in	ADP
cet-3413	9	4	the	the	DET
cet-3413	9	5	near	near	ADJ
cet-3413	9	6	past	past	NOUN
cet-3413	9	7	are	be	AUX
cet-3413	9	8	also	also	ADV
cet-3413	9	9	known	know	VERB
cet-3413	9	10	among	among	ADP
cet-3413	9	11	experts	expert	NOUN
cet-3413	9	12	,	,	PUNCT
cet-3413	9	13	including	include	VERB
cet-3413	9	14	the	the	DET
cet-3413	9	15	reaction	reaction	NOUN
cet-3413	9	16	of	of	ADP
cet-3413	9	17	complex	complex	ADJ
cet-3413	9	18	molecules	molecule	NOUN
cet-3413	9	19	with	with	ADP
cet-3413	9	20	amine	amine	ADJ
cet-3413	9	21	functional	functional	ADJ
cet-3413	9	22	groups	group	NOUN
cet-3413	9	23	with	with	ADP
cet-3413	9	24	dichloromethane	dichloromethane	NOUN
cet-3413	9	25	are	be	AUX
cet-3413	9	26	also	also	ADV
cet-3413	9	27	known	know	VERB
cet-3413	9	28	among	among	ADP
cet-3413	9	29	experts	expert	NOUN
cet-3413	9	30	(	(	PUNCT
cet-3413	9	31	neuenfeld	neuenfeld	ADJ
cet-3413	9	32	,	,	PUNCT
cet-3413	9	33	2008	2008	NUM
cet-3413	9	34	)	)	PUNCT
cet-3413	9	35	.	.	PUNCT
cet-3413	10	1	figure	figure	NOUN
cet-3413	10	2	1	1	NUM
cet-3413	10	3	:	:	PUNCT
cet-3413	10	4	blown	blow	VERB
cet-3413	10	5	up	up	ADP
cet-3413	10	6	waste	waste	NOUN
cet-3413	10	7	drum	drum	NOUN
cet-3413	10	8	with	with	ADP
cet-3413	10	9	dichloromethane	dichloromethane	NOUN
cet-3413	10	10	,	,	PUNCT
cet-3413	10	11	morpholine	morpholine	NOUN
cet-3413	10	12	,	,	PUNCT
cet-3413	10	13	methanol	methanol	NOUN
cet-3413	10	14	as	as	ADP
cet-3413	10	15	main	main	ADJ
cet-3413	10	16	components	component	NOUN
cet-3413	10	17	.	.	PUNCT
cet-3413	11	1	(	(	PUNCT
cet-3413	11	2	neuenfeld	neuenfeld	ADJ
cet-3413	11	3	,	,	PUNCT
cet-3413	11	4	2008	2008	NUM
cet-3413	11	5	)	)	PUNCT
cet-3413	12	1	this	this	PRON
cet-3413	12	2	shows	show	VERB
cet-3413	12	3	that	that	SCONJ
cet-3413	12	4	there	there	PRON
cet-3413	12	5	is	be	VERB
cet-3413	12	6	largely	largely	ADV
cet-3413	12	7	unknown	unknown	ADJ
cet-3413	12	8	potential	potential	ADJ
cet-3413	12	9	risk	risk	NOUN
cet-3413	12	10	,	,	PUNCT
cet-3413	12	11	which	which	PRON
cet-3413	12	12	requires	require	VERB
cet-3413	12	13	a	a	DET
cet-3413	12	14	more	more	ADV
cet-3413	12	15	detailed	detailed	ADJ
cet-3413	12	16	investigation	investigation	NOUN
cet-3413	12	17	.	.	PUNCT
cet-3413	13	1	therefore	therefore	ADV
cet-3413	13	2	the	the	DET
cet-3413	13	3	reaction	reaction	NOUN
cet-3413	13	4	between	between	ADP
cet-3413	13	5	different	different	ADJ
cet-3413	13	6	amine	amine	ADJ
cet-3413	13	7	compounds	compound	NOUN
cet-3413	13	8	and	and	CCONJ
cet-3413	13	9	dichloromethane	dichloromethane	NOUN
cet-3413	13	10	was	be	AUX
cet-3413	13	11	investigated	investigate	VERB
cet-3413	13	12	,	,	PUNCT
cet-3413	13	13	in	in	ADP
cet-3413	13	14	order	order	NOUN
cet-3413	13	15	to	to	PART
cet-3413	13	16	determine	determine	VERB
cet-3413	13	17	the	the	DET
cet-3413	13	18	thermal	thermal	ADJ
cet-3413	13	19	stability	stability	NOUN
cet-3413	13	20	and	and	CCONJ
cet-3413	13	21	the	the	DET
cet-3413	13	22	reactivity	reactivity	NOUN
cet-3413	13	23	of	of	ADP
cet-3413	13	24	the	the	DET
cet-3413	13	25	amine	amine	ADJ
cet-3413	13	26	compounds	compound	NOUN
cet-3413	13	27	toward	toward	ADP
cet-3413	13	28	dichloromethane	dichloromethane	NOUN
cet-3413	13	29	.	.	PUNCT
cet-3413	14	1	the	the	DET
cet-3413	14	2	thermal	thermal	ADJ
cet-3413	14	3	stability	stability	NOUN
cet-3413	14	4	was	be	AUX
cet-3413	14	5	investigated	investigate	VERB
cet-3413	14	6	by	by	ADP
cet-3413	14	7	dsc	dsc	PROPN
cet-3413	14	8	(	(	PUNCT
cet-3413	14	9	differential	differential	NOUN
cet-3413	14	10	scanning	scanning	NOUN
cet-3413	14	11	calorimetry	calorimetry	NOUN
cet-3413	14	12	)	)	PUNCT
cet-3413	14	13	.	.	PUNCT
cet-3413	15	1	for	for	ADP
cet-3413	15	2	this	this	DET
cet-3413	15	3	purpose	purpose	NOUN
cet-3413	15	4	,	,	PUNCT
cet-3413	15	5	different	different	ADJ
cet-3413	15	6	amine	amine	ADJ
cet-3413	15	7	compounds	compound	NOUN
cet-3413	15	8	and	and	CCONJ
cet-3413	15	9	different	different	ADJ
cet-3413	15	10	molar	molar	ADJ
cet-3413	15	11	percentages	percentage	NOUN
cet-3413	15	12	of	of	ADP
cet-3413	15	13	amine	amine	NOUN
cet-3413	15	14	and	and	CCONJ
cet-3413	15	15	dichloromethane	dichloromethane	NOUN
cet-3413	15	16	were	be	AUX
cet-3413	15	17	selected	select	VERB
cet-3413	15	18	.	.	PUNCT
cet-3413	16	1	the	the	DET
cet-3413	16	2	amine	amine	ADJ
cet-3413	16	3	compounds	compound	NOUN
cet-3413	16	4	in	in	ADP
cet-3413	16	5	this	this	DET
cet-3413	16	6	study	study	NOUN
cet-3413	16	7	were	be	AUX
cet-3413	16	8	divided	divide	VERB
cet-3413	16	9	in	in	ADP
cet-3413	16	10	two	two	NUM
cet-3413	16	11	categories	category	NOUN
cet-3413	16	12	:	:	PUNCT
cet-3413	16	13	aliphatic	aliphatic	ADJ
cet-3413	16	14	amines	amine	NOUN
cet-3413	16	15	,	,	PUNCT
cet-3413	16	16	which	which	PRON
cet-3413	16	17	also	also	ADV
cet-3413	16	18	include	include	VERB
cet-3413	16	19	cyclic	cyclic	ADJ
cet-3413	16	20	amines	amine	NOUN
cet-3413	16	21	,	,	PUNCT
cet-3413	16	22	and	and	CCONJ
cet-3413	16	23	aliphatic	aliphatic	ADJ
cet-3413	16	24	-	-	PUNCT
cet-3413	16	25	aromatic	aromatic	ADJ
cet-3413	16	26	amines	amine	NOUN
cet-3413	16	27	.	.	PUNCT
cet-3413	17	1	two	two	NUM
cet-3413	17	2	main	main	ADJ
cet-3413	17	3	variables	variable	NOUN
cet-3413	17	4	were	be	AUX
cet-3413	17	5	first	first	ADV
cet-3413	17	6	compared	compare	VERB
cet-3413	17	7	,	,	PUNCT
cet-3413	17	8	the	the	DET
cet-3413	17	9	onset	onset	NOUN
cet-3413	17	10	of	of	ADP
cet-3413	17	11	the	the	DET
cet-3413	17	12	effect	effect	NOUN
cet-3413	17	13	and	and	CCONJ
cet-3413	17	14	its	its	PRON
cet-3413	17	15	decomposition	decomposition	NOUN
cet-3413	17	16	energy	energy	NOUN
cet-3413	17	17	.	.	PUNCT
cet-3413	18	1	the	the	DET
cet-3413	18	2	investigations	investigation	NOUN
cet-3413	18	3	show	show	VERB
cet-3413	18	4	that	that	SCONJ
cet-3413	18	5	for	for	ADP
cet-3413	18	6	aliphatic	aliphatic	ADJ
cet-3413	18	7	-	-	PUNCT
cet-3413	18	8	aromatic	aromatic	ADJ
cet-3413	18	9	amines	amine	NOUN
cet-3413	18	10	,	,	PUNCT
cet-3413	18	11	the	the	DET
cet-3413	18	12	decomposition	decomposition	NOUN
cet-3413	18	13	energy	energy	NOUN
cet-3413	18	14	decreases	decrease	VERB
cet-3413	18	15	with	with	ADP
cet-3413	18	16	the	the	DET
cet-3413	18	17	molecular	molecular	ADJ
cet-3413	18	18	weight	weight	NOUN
cet-3413	18	19	of	of	ADP
cet-3413	18	20	the	the	DET
cet-3413	18	21	compound	compound	NOUN
cet-3413	18	22	.	.	PUNCT
cet-3413	19	1	cyclic	cyclic	ADJ
cet-3413	19	2	amines	amine	NOUN
cet-3413	19	3	show	show	VERB
cet-3413	19	4	the	the	DET
cet-3413	19	5	highest	high	ADJ
cet-3413	19	6	decomposition	decomposition	NOUN
cet-3413	19	7	energy	energy	NOUN
cet-3413	19	8	,	,	PUNCT
cet-3413	19	9	which	which	PRON
cet-3413	19	10	is	be	AUX
cet-3413	19	11	also	also	ADV
cet-3413	19	12	related	relate	VERB
cet-3413	19	13	with	with	ADP
cet-3413	19	14	the	the	DET
cet-3413	19	15	lowest	low	ADJ
cet-3413	19	16	onset	onset	NOUN
cet-3413	19	17	temperature	temperature	NOUN
cet-3413	19	18	.	.	PUNCT
cet-3413	20	1	the	the	DET
cet-3413	20	2	results	result	NOUN
cet-3413	20	3	show	show	VERB
cet-3413	20	4	significant	significant	ADJ
cet-3413	20	5	decomposition	decomposition	NOUN
cet-3413	20	6	reactions	reaction	NOUN
cet-3413	20	7	in	in	ADP
cet-3413	20	8	ranges	range	NOUN
cet-3413	20	9	of	of	ADP
cet-3413	20	10	the	the	DET
cet-3413	20	11	boiling	boiling	NOUN
cet-3413	20	12	of	of	ADP
cet-3413	20	13	dichloromethane	dichloromethane	NOUN
cet-3413	20	14	.	.	PUNCT
cet-3413	21	1	such	such	ADJ
cet-3413	21	2	reactions	reaction	NOUN
cet-3413	21	3	were	be	AUX
cet-3413	21	4	further	far	ADV
cet-3413	21	5	investigated	investigate	VERB
cet-3413	21	6	using	use	VERB
cet-3413	21	7	different	different	ADJ
cet-3413	21	8	adiabatic	adiabatic	ADJ
cet-3413	21	9	calorimetric	calorimetric	ADJ
cet-3413	21	10	techniques	technique	NOUN
cet-3413	21	11	such	such	ADJ
cet-3413	21	12	as	as	ADP
cet-3413	21	13	vsp2	vsp2	PROPN
cet-3413	21	14	(	(	PUNCT
cet-3413	21	15	vent	vent	NOUN
cet-3413	21	16	sizing	size	VERB
cet-3413	21	17	package	package	NOUN
cet-3413	21	18	)	)	PUNCT
cet-3413	21	19	and	and	CCONJ
cet-3413	21	20	dewar	dewar	ADJ
cet-3413	21	21	calorimetry	calorimetry	NOUN
cet-3413	21	22	.	.	PUNCT
cet-3413	22	1	doi	doi	NOUN
cet-3413	22	2	:	:	PUNCT
cet-3413	22	3	10.3303	10.3303	NUM
cet-3413	22	4	/	/	SYM
cet-3413	22	5	cet1648128	cet1648128	NOUN
cet-3413	22	6	please	please	INTJ
cet-3413	22	7	cite	cite	VERB
cet-3413	22	8	this	this	DET
cet-3413	22	9	article	article	NOUN
cet-3413	22	10	as	as	ADP
cet-3413	22	11	:	:	PUNCT
cet-3413	22	12	dreisch	dreisch	PROPN
cet-3413	22	13	s.	s.	PROPN
cet-3413	22	14	,	,	PUNCT
cet-3413	22	15	hernandez	hernandez	PROPN
cet-3413	22	16	c.	c.	PROPN
cet-3413	22	17	,	,	PUNCT
cet-3413	22	18	horn	horn	PROPN
cet-3413	22	19	j.	j.	PROPN
cet-3413	22	20	,	,	PUNCT
cet-3413	22	21	neuenfeld	neuenfeld	PROPN
cet-3413	22	22	s.	s.	PROPN
cet-3413	22	23	,	,	PUNCT
cet-3413	22	24	2016	2016	NUM
cet-3413	22	25	,	,	PUNCT
cet-3413	22	26	thermal	thermal	ADJ
cet-3413	22	27	stability	stability	NOUN
cet-3413	22	28	of	of	ADP
cet-3413	22	29	amine	amine	ADJ
cet-3413	22	30	compounds	compound	NOUN
cet-3413	22	31	and	and	CCONJ
cet-3413	22	32	dichloromethane	dichloromethane	NOUN
cet-3413	22	33	,	,	PUNCT
cet-3413	22	34	chemical	chemical	ADJ
cet-3413	22	35	engineering	engineering	NOUN
cet-3413	22	36	transactions	transaction	NOUN
cet-3413	22	37	,	,	PUNCT
cet-3413	22	38	48	48	NUM
cet-3413	22	39	,	,	PUNCT
cet-3413	22	40	763	763	NUM
cet-3413	22	41	-	-	SYM
cet-3413	22	42	768	768	NUM
cet-3413	22	43	doi:10.3303	doi:10.3303	NOUN
cet-3413	22	44	/	/	SYM
cet-3413	22	45	cet1648128	cet1648128	NOUN
cet-3413	22	46	763	763	NUM
cet-3413	22	47	1	1	NUM
cet-3413	22	48	.	.	PUNCT
cet-3413	22	49	thermal	thermal	ADJ
cet-3413	22	50	stability	stability	NOUN
cet-3413	22	51	via	via	ADP
cet-3413	22	52	dsc	dsc	NOUN
cet-3413	22	53	(	(	PUNCT
cet-3413	22	54	differential	differential	NOUN
cet-3413	22	55	scanning	scanning	NOUN
cet-3413	22	56	calorimetry	calorimetry	NOUN
cet-3413	22	57	)	)	PUNCT
cet-3413	22	58	the	the	DET
cet-3413	22	59	reaction	reaction	NOUN
cet-3413	22	60	between	between	ADP
cet-3413	22	61	amine	amine	ADJ
cet-3413	22	62	compounds	compound	NOUN
cet-3413	22	63	and	and	CCONJ
cet-3413	22	64	dichloromethane	dichloromethane	NOUN
cet-3413	22	65	was	be	AUX
cet-3413	22	66	investigated	investigate	VERB
cet-3413	22	67	,	,	PUNCT
cet-3413	22	68	in	in	ADP
cet-3413	22	69	order	order	NOUN
cet-3413	22	70	to	to	PART
cet-3413	22	71	determine	determine	VERB
cet-3413	22	72	the	the	DET
cet-3413	22	73	thermal	thermal	ADJ
cet-3413	22	74	stability	stability	NOUN
cet-3413	22	75	and	and	CCONJ
cet-3413	22	76	the	the	DET
cet-3413	22	77	reactivity	reactivity	NOUN
cet-3413	22	78	of	of	ADP
cet-3413	22	79	the	the	DET
cet-3413	22	80	amine	amine	ADJ
cet-3413	22	81	compounds	compound	NOUN
cet-3413	22	82	toward	toward	ADP
cet-3413	22	83	dichloromethane	dichloromethane	NOUN
cet-3413	22	84	.	.	PUNCT
cet-3413	23	1	the	the	DET
cet-3413	23	2	thermal	thermal	ADJ
cet-3413	23	3	stability	stability	NOUN
cet-3413	23	4	was	be	AUX
cet-3413	23	5	first	first	ADV
cet-3413	23	6	investigated	investigate	VERB
cet-3413	23	7	by	by	ADP
cet-3413	23	8	dsc	dsc	PROPN
cet-3413	23	9	(	(	PUNCT
cet-3413	23	10	differential	differential	NOUN
cet-3413	23	11	scanning	scanning	NOUN
cet-3413	23	12	calorimetry	calorimetry	NOUN
cet-3413	23	13	)	)	PUNCT
cet-3413	23	14	.	.	PUNCT
cet-3413	24	1	for	for	ADP
cet-3413	24	2	this	this	DET
cet-3413	24	3	purpose	purpose	NOUN
cet-3413	24	4	,	,	PUNCT
cet-3413	24	5	a	a	DET
cet-3413	24	6	small	small	ADJ
cet-3413	24	7	amount	amount	NOUN
cet-3413	24	8	(	(	PUNCT
cet-3413	24	9	about	about	ADV
cet-3413	24	10	10	10	NUM
cet-3413	24	11	mg	mg	NOUN
cet-3413	24	12	)	)	PUNCT
cet-3413	24	13	of	of	ADP
cet-3413	24	14	sample	sample	NOUN
cet-3413	24	15	was	be	AUX
cet-3413	24	16	weighed	weigh	VERB
cet-3413	24	17	into	into	ADP
cet-3413	24	18	a	a	DET
cet-3413	24	19	crucible	crucible	NOUN
cet-3413	24	20	.	.	PUNCT
cet-3413	25	1	the	the	DET
cet-3413	25	2	sample	sample	NOUN
cet-3413	25	3	was	be	AUX
cet-3413	25	4	measured	measure	VERB
cet-3413	25	5	against	against	ADP
cet-3413	25	6	a	a	DET
cet-3413	25	7	crucible	crucible	NOUN
cet-3413	25	8	of	of	ADP
cet-3413	25	9	same	same	ADJ
cet-3413	25	10	material	material	NOUN
cet-3413	25	11	filled	fill	VERB
cet-3413	25	12	with	with	ADP
cet-3413	25	13	aluminium	aluminium	NOUN
cet-3413	25	14	oxide	oxide	NOUN
cet-3413	25	15	as	as	ADP
cet-3413	25	16	reference	reference	NOUN
cet-3413	25	17	.	.	PUNCT
cet-3413	26	1	the	the	DET
cet-3413	26	2	crucibles	crucible	NOUN
cet-3413	26	3	were	be	AUX
cet-3413	26	4	then	then	ADV
cet-3413	26	5	placed	place	VERB
cet-3413	26	6	in	in	ADP
cet-3413	26	7	the	the	DET
cet-3413	26	8	equipment	equipment	NOUN
cet-3413	26	9	dsc-1	dsc-1	NOUN
cet-3413	26	10	star	star	NOUN
cet-3413	26	11	dsc	dsc	PROPN
cet-3413	26	12	of	of	ADP
cet-3413	26	13	mettlertoledo	mettlertoledo	PROPN
cet-3413	26	14	and	and	CCONJ
cet-3413	26	15	heated	heat	VERB
cet-3413	26	16	at	at	ADP
cet-3413	26	17	a	a	DET
cet-3413	26	18	rate	rate	NOUN
cet-3413	26	19	of	of	ADP
cet-3413	26	20	3	3	NUM
cet-3413	26	21	k	k	NOUN
cet-3413	26	22	/	/	SYM
cet-3413	26	23	min	min	NOUN
cet-3413	26	24	to	to	PART
cet-3413	26	25	record	record	VERB
cet-3413	26	26	the	the	DET
cet-3413	26	27	thermal	thermal	ADJ
cet-3413	26	28	trace	trace	NOUN
cet-3413	26	29	of	of	ADP
cet-3413	26	30	the	the	DET
cet-3413	26	31	mixture	mixture	NOUN
cet-3413	26	32	.	.	PUNCT
cet-3413	27	1	different	different	ADJ
cet-3413	27	2	amine	amine	ADJ
cet-3413	27	3	compounds	compound	NOUN
cet-3413	27	4	and	and	CCONJ
cet-3413	27	5	different	different	ADJ
cet-3413	27	6	molar	molar	ADJ
cet-3413	27	7	percentages	percentage	NOUN
cet-3413	27	8	of	of	ADP
cet-3413	27	9	amine	amine	NOUN
cet-3413	27	10	and	and	CCONJ
cet-3413	27	11	dichloromethane	dichloromethane	NOUN
cet-3413	27	12	were	be	AUX
cet-3413	27	13	selected	select	VERB
cet-3413	27	14	.	.	PUNCT
cet-3413	28	1	the	the	DET
cet-3413	28	2	amine	amine	ADJ
cet-3413	28	3	compounds	compound	NOUN
cet-3413	28	4	in	in	ADP
cet-3413	28	5	this	this	DET
cet-3413	28	6	study	study	NOUN
cet-3413	28	7	were	be	AUX
cet-3413	28	8	divided	divide	VERB
cet-3413	28	9	in	in	ADP
cet-3413	28	10	two	two	NUM
cet-3413	28	11	categories	category	NOUN
cet-3413	28	12	:	:	PUNCT
cet-3413	28	13	aliphatic	aliphatic	ADJ
cet-3413	28	14	amines	amine	NOUN
cet-3413	28	15	and	and	CCONJ
cet-3413	28	16	aliphatic	aliphatic	ADJ
cet-3413	28	17	-	-	PUNCT
cet-3413	28	18	aromatic	aromatic	ADJ
cet-3413	28	19	amines	amine	NOUN
cet-3413	28	20	.	.	PUNCT
cet-3413	29	1	two	two	NUM
cet-3413	29	2	main	main	ADJ
cet-3413	29	3	variables	variable	NOUN
cet-3413	29	4	were	be	AUX
cet-3413	29	5	first	first	ADV
cet-3413	29	6	compared	compare	VERB
cet-3413	29	7	,	,	PUNCT
cet-3413	29	8	the	the	DET
cet-3413	29	9	onset	onset	NOUN
cet-3413	29	10	of	of	ADP
cet-3413	29	11	the	the	DET
cet-3413	29	12	effect	effect	NOUN
cet-3413	29	13	and	and	CCONJ
cet-3413	29	14	its	its	PRON
cet-3413	29	15	decomposition	decomposition	NOUN
cet-3413	29	16	energy	energy	NOUN
cet-3413	29	17	.	.	PUNCT
cet-3413	30	1	for	for	ADP
cet-3413	30	2	comparison	comparison	NOUN
cet-3413	30	3	of	of	ADP
cet-3413	30	4	the	the	DET
cet-3413	30	5	results	result	NOUN
cet-3413	30	6	the	the	DET
cet-3413	30	7	molar	molar	ADJ
cet-3413	30	8	percentages	percentage	NOUN
cet-3413	30	9	are	be	AUX
cet-3413	30	10	plotted	plot	VERB
cet-3413	30	11	against	against	ADP
cet-3413	30	12	the	the	DET
cet-3413	30	13	decomposition	decomposition	NOUN
cet-3413	30	14	energy	energy	NOUN
cet-3413	30	15	for	for	ADP
cet-3413	30	16	both	both	DET
cet-3413	30	17	categories	category	NOUN
cet-3413	30	18	in	in	ADP
cet-3413	30	19	figures	figure	NOUN
cet-3413	30	20	2	2	NUM
cet-3413	30	21	and	and	CCONJ
cet-3413	30	22	3	3	NUM
cet-3413	30	23	.	.	X
cet-3413	30	24	figure	figure	NOUN
cet-3413	30	25	2	2	NUM
cet-3413	30	26	:	:	PUNCT
cet-3413	30	27	molar	molar	ADJ
cet-3413	30	28	percentages	percentage	NOUN
cet-3413	30	29	of	of	ADP
cet-3413	30	30	aliphatic	aliphatic	ADJ
cet-3413	30	31	amines	amine	NOUN
cet-3413	30	32	in	in	ADP
cet-3413	30	33	dichloromethane	dichloromethane	NOUN
cet-3413	30	34	vs	vs	ADP
cet-3413	30	35	energy	energy	NOUN
cet-3413	30	36	of	of	ADP
cet-3413	30	37	the	the	DET
cet-3413	30	38	decomposition	decomposition	NOUN
cet-3413	30	39	figure	figure	NOUN
cet-3413	30	40	3	3	NUM
cet-3413	30	41	:	:	PUNCT
cet-3413	30	42	molar	molar	ADJ
cet-3413	30	43	percentages	percentage	NOUN
cet-3413	30	44	of	of	ADP
cet-3413	30	45	aliphatic	aliphatic	ADJ
cet-3413	30	46	-	-	PUNCT
cet-3413	30	47	aromatic	aromatic	ADJ
cet-3413	30	48	amines	amine	NOUN
cet-3413	30	49	in	in	ADP
cet-3413	30	50	dichloromethane	dichloromethane	NOUN
cet-3413	30	51	vs	vs	ADP
cet-3413	30	52	energy	energy	NOUN
cet-3413	30	53	of	of	ADP
cet-3413	30	54	the	the	DET
cet-3413	30	55	decomposition	decomposition	NOUN
cet-3413	30	56	0	0	NUM
cet-3413	31	1	100	100	NUM
cet-3413	31	2	200	200	NUM
cet-3413	31	3	300	300	NUM
cet-3413	31	4	400	400	NUM
cet-3413	31	5	500	500	NUM
cet-3413	31	6	600	600	NUM
cet-3413	31	7	700	700	NUM
cet-3413	31	8	800	800	NUM
cet-3413	31	9	900	900	NUM
cet-3413	31	10	1.000	1.000	NUM
cet-3413	31	11	1.100	1.100	NUM
cet-3413	31	12	1.200	1.200	NUM
cet-3413	31	13	30	30	NUM
cet-3413	31	14	35	35	NUM
cet-3413	31	15	40	40	NUM
cet-3413	31	16	45	45	NUM
cet-3413	31	17	50	50	NUM
cet-3413	31	18	55	55	NUM
cet-3413	31	19	60	60	NUM
cet-3413	31	20	65	65	NUM
cet-3413	31	21	70	70	NUM
cet-3413	31	22	75	75	NUM
cet-3413	31	23	80	80	NUM
cet-3413	31	24	85	85	NUM
cet-3413	31	25	en	en	INTJ
cet-3413	31	26	er	er	INTJ
cet-3413	31	27	gy	gy	NOUN
cet-3413	31	28	o	o	NOUN
cet-3413	31	29	f	f	PROPN
cet-3413	31	30	d	d	X
cet-3413	31	31	ec	ec	PROPN
cet-3413	31	32	om	om	PROPN
cet-3413	31	33	po	po	NOUN
cet-3413	31	34	si	si	PROPN
cet-3413	31	35	tio	tio	PROPN
cet-3413	31	36	n	n	PROPN
cet-3413	31	37	(	(	PUNCT
cet-3413	31	38	j	j	PROPN
cet-3413	31	39	/g	/g	PUNCT
cet-3413	31	40	)	)	PUNCT
cet-3413	32	1	%	%	INTJ
cet-3413	32	2	molar	molar	ADJ
cet-3413	32	3	amine	amine	NOUN
cet-3413	32	4	in	in	ADP
cet-3413	32	5	dichloromethane	dichloromethane	NOUN
cet-3413	32	6	pyrrolidine	pyrrolidine	ADJ
cet-3413	32	7	piperidine	piperidine	NOUN
cet-3413	32	8	morpholine	morpholine	ADJ
cet-3413	32	9	hexylamine	hexylamine	NOUN
cet-3413	32	10	dipropylamine	dipropylamine	NOUN
cet-3413	32	11	trimethylamine	trimethylamine	NOUN
cet-3413	32	12	triethylamine	triethylamine	NOUN
cet-3413	32	13	trihexylamine	trihexylamine	NOUN
cet-3413	32	14	30	30	NUM
cet-3413	32	15	35	35	NUM
cet-3413	32	16	40	40	NUM
cet-3413	32	17	45	45	NUM
cet-3413	32	18	50	50	NUM
cet-3413	32	19	55	55	NUM
cet-3413	32	20	60	60	NUM
cet-3413	32	21	65	65	NUM
cet-3413	32	22	70	70	NUM
cet-3413	32	23	75	75	NUM
cet-3413	32	24	80	80	NUM
cet-3413	32	25	85	85	NUM
cet-3413	32	26	0	0	NUM
cet-3413	32	27	100	100	NUM
cet-3413	32	28	200	200	NUM
cet-3413	32	29	300	300	NUM
cet-3413	32	30	400	400	NUM
cet-3413	32	31	500	500	NUM
cet-3413	32	32	600	600	NUM
cet-3413	32	33	700	700	NUM
cet-3413	32	34	800	800	NUM
cet-3413	32	35	900	900	NUM
cet-3413	32	36	%	%	NOUN
cet-3413	32	37	molar	molar	ADJ
cet-3413	32	38	amine	amine	NOUN
cet-3413	32	39	in	in	ADP
cet-3413	32	40	dichloromethane	dichloromethane	NOUN
cet-3413	32	41	en	en	PROPN
cet-3413	32	42	er	er	INTJ
cet-3413	32	43	gy	gy	NOUN
cet-3413	32	44	o	o	NOUN
cet-3413	32	45	f	f	PROPN
cet-3413	33	1	d	d	X
cet-3413	33	2	ec	ec	PROPN
cet-3413	33	3	om	om	PROPN
cet-3413	33	4	po	po	NOUN
cet-3413	33	5	si	si	PROPN
cet-3413	33	6	tio	tio	PROPN
cet-3413	33	7	n	n	PROPN
cet-3413	33	8	(	(	PUNCT
cet-3413	33	9	j	j	PROPN
cet-3413	33	10	/g	/g	PUNCT
cet-3413	33	11	)	)	PUNCT
cet-3413	33	12	aniline	aniline	NOUN
cet-3413	33	13	benzylamine	benzylamine	NOUN
cet-3413	33	14	benzyl(methyl)amine	benzyl(methyl)amine	PROPN
cet-3413	33	15	benzyl(dimethyl)amine	benzyl(dimethyl)amine	PROPN
cet-3413	33	16	764	764	NUM
cet-3413	33	17	in	in	ADP
cet-3413	33	18	addition	addition	NOUN
cet-3413	33	19	,	,	PUNCT
cet-3413	33	20	all	all	DET
cet-3413	33	21	amine	amine	ADJ
cet-3413	33	22	compounds	compound	NOUN
cet-3413	33	23	and	and	CCONJ
cet-3413	33	24	dichloromethane	dichloromethane	NOUN
cet-3413	33	25	were	be	AUX
cet-3413	33	26	investigated	investigate	VERB
cet-3413	33	27	separately	separately	ADV
cet-3413	33	28	.	.	PUNCT
cet-3413	34	1	the	the	DET
cet-3413	34	2	raw	raw	ADJ
cet-3413	34	3	materials	material	NOUN
cet-3413	34	4	showed	show	VERB
cet-3413	34	5	no	no	DET
cet-3413	34	6	significant	significant	ADJ
cet-3413	34	7	thermal	thermal	ADJ
cet-3413	34	8	effects	effect	NOUN
cet-3413	34	9	in	in	ADP
cet-3413	34	10	the	the	DET
cet-3413	34	11	dsc	dsc	NOUN
cet-3413	34	12	measurements	measurement	NOUN
cet-3413	34	13	.	.	PUNCT
cet-3413	35	1	due	due	ADP
cet-3413	35	2	to	to	ADP
cet-3413	35	3	this	this	DET
cet-3413	35	4	result	result	NOUN
cet-3413	35	5	,	,	PUNCT
cet-3413	35	6	it	it	PRON
cet-3413	35	7	can	can	AUX
cet-3413	35	8	be	be	AUX
cet-3413	35	9	stated	state	VERB
cet-3413	35	10	that	that	SCONJ
cet-3413	35	11	the	the	DET
cet-3413	35	12	observed	observed	ADJ
cet-3413	35	13	exothermic	exothermic	ADJ
cet-3413	35	14	effects	effect	NOUN
cet-3413	35	15	of	of	ADP
cet-3413	35	16	the	the	DET
cet-3413	35	17	mixtures	mixture	NOUN
cet-3413	35	18	can	can	AUX
cet-3413	35	19	be	be	AUX
cet-3413	35	20	assigned	assign	VERB
cet-3413	35	21	to	to	ADP
cet-3413	35	22	the	the	DET
cet-3413	35	23	reaction	reaction	NOUN
cet-3413	35	24	between	between	ADP
cet-3413	35	25	the	the	DET
cet-3413	35	26	amine	amine	ADJ
cet-3413	35	27	compounds	compound	NOUN
cet-3413	35	28	and	and	CCONJ
cet-3413	35	29	dichloromethane	dichloromethane	NOUN
cet-3413	35	30	.	.	PUNCT
cet-3413	36	1	the	the	DET
cet-3413	36	2	results	result	NOUN
cet-3413	36	3	show	show	VERB
cet-3413	36	4	a	a	DET
cet-3413	36	5	maximum	maximum	NOUN
cet-3413	36	6	regarding	regard	VERB
cet-3413	36	7	the	the	DET
cet-3413	36	8	decomposition	decomposition	NOUN
cet-3413	36	9	energy	energy	NOUN
cet-3413	36	10	for	for	ADP
cet-3413	36	11	a	a	DET
cet-3413	36	12	mixture	mixture	NOUN
cet-3413	36	13	of	of	ADP
cet-3413	36	14	amine	amine	NOUN
cet-3413	36	15	/	/	SYM
cet-3413	36	16	dichloromethane	dichloromethane	NOUN
cet-3413	36	17	with	with	ADP
cet-3413	36	18	a	a	DET
cet-3413	36	19	ratio	ratio	NOUN
cet-3413	36	20	of	of	ADP
cet-3413	36	21	2:1	2:1	NUM
cet-3413	36	22	.	.	PUNCT
cet-3413	37	1	this	this	DET
cet-3413	37	2	statement	statement	NOUN
cet-3413	37	3	applies	apply	VERB
cet-3413	37	4	to	to	ADP
cet-3413	37	5	all	all	DET
cet-3413	37	6	cases	case	NOUN
cet-3413	37	7	except	except	SCONJ
cet-3413	37	8	for	for	ADP
cet-3413	37	9	trihexylamine	trihexylamine	PRON
cet-3413	37	10	.	.	PUNCT
cet-3413	38	1	this	this	DET
cet-3413	38	2	compound	compound	NOUN
cet-3413	38	3	shows	show	VERB
cet-3413	38	4	a	a	DET
cet-3413	38	5	very	very	ADV
cet-3413	38	6	low	low	ADJ
cet-3413	38	7	decomposition	decomposition	NOUN
cet-3413	38	8	energy	energy	NOUN
cet-3413	38	9	reaching	reach	VERB
cet-3413	38	10	a	a	DET
cet-3413	38	11	value	value	NOUN
cet-3413	38	12	of	of	ADP
cet-3413	38	13	approx	approx	PROPN
cet-3413	38	14	.	.	PUNCT
cet-3413	39	1	100	100	NUM
cet-3413	39	2	j	j	PROPN
cet-3413	39	3	/	/	SYM
cet-3413	39	4	g	g	NOUN
cet-3413	39	5	for	for	ADP
cet-3413	39	6	a	a	DET
cet-3413	39	7	2:1	2:1	NUM
cet-3413	39	8	mixture	mixture	NOUN
cet-3413	39	9	,	,	PUNCT
cet-3413	39	10	which	which	PRON
cet-3413	39	11	can	can	AUX
cet-3413	39	12	not	not	PART
cet-3413	39	13	be	be	AUX
cet-3413	39	14	considered	consider	VERB
cet-3413	39	15	to	to	PART
cet-3413	39	16	have	have	VERB
cet-3413	39	17	any	any	DET
cet-3413	39	18	significance	significance	NOUN
cet-3413	39	19	.	.	PUNCT
cet-3413	40	1	the	the	DET
cet-3413	40	2	decomposition	decomposition	NOUN
cet-3413	40	3	energy	energy	NOUN
cet-3413	40	4	and	and	CCONJ
cet-3413	40	5	onset	onset	VERB
cet-3413	40	6	temperature	temperature	NOUN
cet-3413	40	7	of	of	ADP
cet-3413	40	8	the	the	DET
cet-3413	40	9	obtained	obtain	VERB
cet-3413	40	10	results	result	NOUN
cet-3413	40	11	for	for	ADP
cet-3413	40	12	a	a	DET
cet-3413	40	13	mixture	mixture	NOUN
cet-3413	40	14	of	of	ADP
cet-3413	40	15	amine	amine	NOUN
cet-3413	40	16	/	/	SYM
cet-3413	40	17	dichloromethane	dichloromethane	NOUN
cet-3413	40	18	with	with	ADP
cet-3413	40	19	a	a	DET
cet-3413	40	20	ratio	ratio	NOUN
cet-3413	40	21	of	of	ADP
cet-3413	40	22	2:1	2:1	NUM
cet-3413	40	23	are	be	AUX
cet-3413	40	24	compared	compare	VERB
cet-3413	40	25	and	and	CCONJ
cet-3413	40	26	listed	list	VERB
cet-3413	40	27	in	in	ADP
cet-3413	40	28	table	table	NOUN
cet-3413	40	29	1	1	NUM
cet-3413	40	30	and	and	CCONJ
cet-3413	40	31	2	2	NUM
cet-3413	40	32	.	.	NOUN
cet-3413	40	33	table	table	NOUN
cet-3413	40	34	1	1	NUM
cet-3413	40	35	:	:	PUNCT
cet-3413	40	36	energy	energy	NOUN
cet-3413	40	37	and	and	CCONJ
cet-3413	40	38	onset	onset	ADJ
cet-3413	40	39	temperature	temperature	NOUN
cet-3413	40	40	of	of	ADP
cet-3413	40	41	the	the	DET
cet-3413	40	42	decomposition	decomposition	NOUN
cet-3413	40	43	for	for	ADP
cet-3413	40	44	aliphatic	aliphatic	ADJ
cet-3413	40	45	amines	amine	NOUN
cet-3413	40	46	in	in	ADP
cet-3413	40	47	dichloromethane	dichloromethane	NOUN
cet-3413	40	48	with	with	ADP
cet-3413	40	49	ratios	ratio	NOUN
cet-3413	40	50	of	of	ADP
cet-3413	40	51	2:1	2:1	NUM
cet-3413	40	52	type	type	NOUN
cet-3413	40	53	compound	compound	NOUN
cet-3413	40	54	molecular	molecular	ADJ
cet-3413	40	55	weight	weight	NOUN
cet-3413	40	56	(	(	PUNCT
cet-3413	40	57	g	g	NOUN
cet-3413	40	58	/	/	SYM
cet-3413	40	59	mol	mol	NOUN
cet-3413	40	60	)	)	PUNCT
cet-3413	40	61	energy	energy	NOUN
cet-3413	40	62	of	of	ADP
cet-3413	40	63	decomposition	decomposition	NOUN
cet-3413	40	64	(	(	PUNCT
cet-3413	40	65	j	j	NOUN
cet-3413	40	66	/	/	SYM
cet-3413	40	67	g	g	NOUN
cet-3413	40	68	)	)	PUNCT
cet-3413	40	69	tonset	tonset	NOUN
cet-3413	40	70	(	(	PUNCT
cet-3413	40	71	°	°	ADP
cet-3413	40	72	c	c	NOUN
cet-3413	40	73	)	)	PUNCT
cet-3413	40	74	secondary	secondary	ADJ
cet-3413	40	75	(	(	PUNCT
cet-3413	40	76	cyclic	cyclic	ADJ
cet-3413	40	77	)	)	PUNCT
cet-3413	40	78	pyrrolidine	pyrrolidine	NOUN
cet-3413	40	79	71.12	71.12	NUM
cet-3413	40	80	1030	1030	NUM
cet-3413	40	81	40	40	NUM
cet-3413	40	82	piperidine	piperidine	NOUN
cet-3413	40	83	85.15	85.15	NUM
cet-3413	40	84	1080	1080	NUM
cet-3413	40	85	40	40	NUM
cet-3413	40	86	morpholine	morpholine	NOUN
cet-3413	40	87	87.10	87.10	NUM
cet-3413	40	88	1000	1000	NUM
cet-3413	40	89	50	50	NUM
cet-3413	40	90	primary	primary	ADJ
cet-3413	40	91	hexylamine	hexylamine	NOUN
cet-3413	41	1	101.19	101.19	NUM
cet-3413	41	2	830	830	NUM
cet-3413	41	3	110	110	NUM
cet-3413	41	4	secondary	secondary	ADJ
cet-3413	41	5	dipropylamine	dipropylamine	NOUN
cet-3413	41	6	101.19	101.19	NUM
cet-3413	41	7	790	790	NUM
cet-3413	41	8	130	130	NUM
cet-3413	41	9	tertiary	tertiary	ADJ
cet-3413	41	10	trimethylamine	trimethylamine	NOUN
cet-3413	41	11	59.11	59.11	NUM
cet-3413	41	12	520	520	NUM
cet-3413	41	13	210	210	NUM
cet-3413	41	14	triethylamine	triethylamine	NOUN
cet-3413	41	15	101.19	101.19	NUM
cet-3413	41	16	890	890	NUM
cet-3413	41	17	180	180	NUM
cet-3413	41	18	trihexylamine	trihexylamine	NUM
cet-3413	41	19	269.51	269.51	NUM
cet-3413	41	20	150	150	NUM
cet-3413	41	21	210	210	NUM
cet-3413	41	22	comparing	compare	VERB
cet-3413	41	23	the	the	DET
cet-3413	41	24	aliphatic	aliphatic	ADJ
cet-3413	41	25	amines	amine	NOUN
cet-3413	41	26	,	,	PUNCT
cet-3413	41	27	the	the	DET
cet-3413	41	28	cyclic	cyclic	ADJ
cet-3413	41	29	amines	amine	NOUN
cet-3413	41	30	show	show	VERB
cet-3413	41	31	the	the	DET
cet-3413	41	32	highest	high	ADJ
cet-3413	41	33	decomposition	decomposition	NOUN
cet-3413	41	34	energy	energy	NOUN
cet-3413	41	35	,	,	PUNCT
cet-3413	41	36	which	which	PRON
cet-3413	41	37	is	be	AUX
cet-3413	41	38	also	also	ADV
cet-3413	41	39	related	relate	VERB
cet-3413	41	40	to	to	ADP
cet-3413	41	41	the	the	DET
cet-3413	41	42	lowest	low	ADJ
cet-3413	41	43	onset	onset	ADJ
cet-3413	41	44	temperature	temperature	NOUN
cet-3413	41	45	.	.	PUNCT
cet-3413	42	1	for	for	ADP
cet-3413	42	2	the	the	DET
cet-3413	42	3	non	non	ADJ
cet-3413	42	4	-	-	ADJ
cet-3413	42	5	cyclic	cyclic	ADJ
cet-3413	42	6	aliphatic	aliphatic	ADJ
cet-3413	42	7	amines	amine	NOUN
cet-3413	42	8	,	,	PUNCT
cet-3413	42	9	the	the	DET
cet-3413	42	10	decomposition	decomposition	NOUN
cet-3413	42	11	energy	energy	NOUN
cet-3413	42	12	decreases	decrease	VERB
cet-3413	42	13	with	with	ADP
cet-3413	42	14	the	the	DET
cet-3413	42	15	substitution	substitution	NOUN
cet-3413	42	16	pattern	pattern	NOUN
cet-3413	42	17	(	(	PUNCT
cet-3413	42	18	primary	primary	ADJ
cet-3413	42	19	>	>	X
cet-3413	42	20	secondary	secondary	ADJ
cet-3413	42	21	>	>	X
cet-3413	42	22	tertiary	tertiary	NOUN
cet-3413	42	23	)	)	PUNCT
cet-3413	42	24	.	.	PUNCT
cet-3413	43	1	the	the	DET
cet-3413	43	2	onset	onset	NOUN
cet-3413	43	3	temperature	temperature	NOUN
cet-3413	43	4	of	of	ADP
cet-3413	43	5	the	the	DET
cet-3413	43	6	effect	effect	NOUN
cet-3413	43	7	decreases	decrease	VERB
cet-3413	43	8	with	with	ADP
cet-3413	43	9	an	an	DET
cet-3413	43	10	increasing	increase	VERB
cet-3413	43	11	decomposition	decomposition	NOUN
cet-3413	43	12	energy	energy	NOUN
cet-3413	43	13	.	.	PUNCT
cet-3413	44	1	table	table	NOUN
cet-3413	44	2	2	2	NUM
cet-3413	44	3	:	:	PUNCT
cet-3413	44	4	energy	energy	NOUN
cet-3413	44	5	and	and	CCONJ
cet-3413	44	6	onset	onset	ADJ
cet-3413	44	7	temperature	temperature	NOUN
cet-3413	44	8	of	of	ADP
cet-3413	44	9	the	the	DET
cet-3413	44	10	decomposition	decomposition	NOUN
cet-3413	44	11	of	of	ADP
cet-3413	44	12	aliphatic	aliphatic	ADJ
cet-3413	44	13	-	-	PUNCT
cet-3413	44	14	aromatic	aromatic	ADJ
cet-3413	44	15	amines	amine	NOUN
cet-3413	44	16	in	in	ADP
cet-3413	44	17	dichloromethane	dichloromethane	NOUN
cet-3413	44	18	with	with	ADP
cet-3413	44	19	ratios	ratio	NOUN
cet-3413	44	20	of	of	ADP
cet-3413	44	21	2:1	2:1	NUM
cet-3413	44	22	type	type	NOUN
cet-3413	44	23	compound	compound	NOUN
cet-3413	44	24	molecular	molecular	ADJ
cet-3413	44	25	weight	weight	NOUN
cet-3413	44	26	(	(	PUNCT
cet-3413	44	27	g	g	NOUN
cet-3413	44	28	/	/	SYM
cet-3413	44	29	mol	mol	NOUN
cet-3413	44	30	)	)	PUNCT
cet-3413	44	31	energy	energy	NOUN
cet-3413	44	32	of	of	ADP
cet-3413	44	33	decomposition	decomposition	NOUN
cet-3413	44	34	(	(	PUNCT
cet-3413	44	35	j	j	NOUN
cet-3413	44	36	/	/	SYM
cet-3413	44	37	g	g	NOUN
cet-3413	44	38	)	)	PUNCT
cet-3413	44	39	tonset	tonset	NOUN
cet-3413	44	40	(	(	PUNCT
cet-3413	44	41	°	°	ADP
cet-3413	44	42	c	c	NOUN
cet-3413	44	43	)	)	PUNCT
cet-3413	44	44	primary	primary	ADJ
cet-3413	44	45	aniline	aniline	NOUN
cet-3413	44	46	93.13	93.13	NUM
cet-3413	44	47	800	800	NUM
cet-3413	44	48	130	130	NUM
cet-3413	44	49	benzylamine	benzylamine	NOUN
cet-3413	44	50	107.15	107.15	NUM
cet-3413	44	51	840	840	NUM
cet-3413	44	52	100	100	NUM
cet-3413	44	53	secondary	secondary	ADJ
cet-3413	44	54	benzyl(methyl)amine	benzyl(methyl)amine	PROPN
cet-3413	44	55	121.18	121.18	NUM
cet-3413	44	56	700	700	NUM
cet-3413	44	57	80	80	NUM
cet-3413	44	58	tertiary	tertiary	ADJ
cet-3413	44	59	benzyl(dimethyl)amine	benzyl(dimethyl)amine	NOUN
cet-3413	44	60	135.21	135.21	NUM
cet-3413	44	61	540	540	NUM
cet-3413	44	62	130	130	NUM
cet-3413	44	63	for	for	ADP
cet-3413	44	64	the	the	DET
cet-3413	44	65	aliphatic	aliphatic	ADJ
cet-3413	44	66	-	-	PUNCT
cet-3413	44	67	aromatic	aromatic	ADJ
cet-3413	44	68	amines	amine	NOUN
cet-3413	44	69	,	,	PUNCT
cet-3413	44	70	it	it	PRON
cet-3413	44	71	can	can	AUX
cet-3413	44	72	be	be	AUX
cet-3413	44	73	observed	observe	VERB
cet-3413	44	74	that	that	SCONJ
cet-3413	44	75	the	the	DET
cet-3413	44	76	energy	energy	NOUN
cet-3413	44	77	of	of	ADP
cet-3413	44	78	the	the	DET
cet-3413	44	79	exothermic	exothermic	ADJ
cet-3413	44	80	effect	effect	NOUN
cet-3413	44	81	decreases	decrease	VERB
cet-3413	44	82	with	with	ADP
cet-3413	44	83	the	the	DET
cet-3413	44	84	molecular	molecular	ADJ
cet-3413	44	85	weight	weight	NOUN
cet-3413	44	86	of	of	ADP
cet-3413	44	87	the	the	DET
cet-3413	44	88	compound	compound	NOUN
cet-3413	44	89	and	and	CCONJ
cet-3413	44	90	also	also	ADV
cet-3413	44	91	decreases	decrease	VERB
cet-3413	44	92	with	with	ADP
cet-3413	44	93	the	the	DET
cet-3413	44	94	substitution	substitution	NOUN
cet-3413	44	95	pattern	pattern	NOUN
cet-3413	44	96	.	.	PUNCT
cet-3413	45	1	the	the	DET
cet-3413	45	2	decomposition	decomposition	NOUN
cet-3413	45	3	of	of	ADP
cet-3413	45	4	morpholine	morpholine	NOUN
cet-3413	45	5	in	in	ADP
cet-3413	45	6	dichloromethane	dichloromethane	NOUN
cet-3413	45	7	was	be	AUX
cet-3413	45	8	further	far	ADV
cet-3413	45	9	investigated	investigate	VERB
cet-3413	45	10	by	by	ADP
cet-3413	45	11	s.	s.	PROPN
cet-3413	45	12	neuenfeld	neuenfeld	PROPN
cet-3413	45	13	in	in	ADP
cet-3413	45	14	2008	2008	NUM
cet-3413	45	15	.	.	PUNCT
cet-3413	46	1	figure	figure	NOUN
cet-3413	46	2	4	4	NUM
cet-3413	46	3	shows	show	VERB
cet-3413	46	4	an	an	DET
cet-3413	46	5	ftir	ftir	ADJ
cet-3413	46	6	analysis	analysis	NOUN
cet-3413	46	7	of	of	ADP
cet-3413	46	8	the	the	DET
cet-3413	46	9	starting	start	VERB
cet-3413	46	10	materials	material	NOUN
cet-3413	46	11	and	and	CCONJ
cet-3413	46	12	the	the	DET
cet-3413	46	13	reaction	reaction	NOUN
cet-3413	46	14	product	product	NOUN
cet-3413	46	15	,	,	PUNCT
cet-3413	46	16	showing	show	VERB
cet-3413	46	17	that	that	DET
cet-3413	46	18	variety	variety	NOUN
cet-3413	46	19	of	of	ADP
cet-3413	46	20	products	product	NOUN
cet-3413	46	21	is	be	AUX
cet-3413	46	22	formed	form	VERB
cet-3413	46	23	during	during	ADP
cet-3413	46	24	the	the	DET
cet-3413	46	25	decomposition	decomposition	NOUN
cet-3413	46	26	.	.	PUNCT
cet-3413	47	1	figure	figure	NOUN
cet-3413	47	2	4	4	NUM
cet-3413	47	3	:	:	PUNCT
cet-3413	47	4	ftir	ftir	VERB
cet-3413	47	5	analysis	analysis	NOUN
cet-3413	47	6	of	of	ADP
cet-3413	47	7	the	the	DET
cet-3413	47	8	starting	start	VERB
cet-3413	47	9	materials	material	NOUN
cet-3413	47	10	and	and	CCONJ
cet-3413	47	11	reaction	reaction	NOUN
cet-3413	47	12	product	product	NOUN
cet-3413	47	13	of	of	ADP
cet-3413	47	14	morphopline	morphopline	NOUN
cet-3413	47	15	in	in	ADP
cet-3413	47	16	dichloromethane	dichloromethane	NOUN
cet-3413	47	17	(	(	PUNCT
cet-3413	47	18	neuenfeld	neuenfeld	ADJ
cet-3413	47	19	,	,	PUNCT
cet-3413	47	20	2008	2008	NUM
cet-3413	47	21	)	)	PUNCT
cet-3413	47	22	765	765	NUM
cet-3413	47	23	this	this	PRON
cet-3413	47	24	leads	lead	VERB
cet-3413	47	25	to	to	ADP
cet-3413	47	26	the	the	DET
cet-3413	47	27	assumption	assumption	NOUN
cet-3413	47	28	of	of	ADP
cet-3413	47	29	a	a	DET
cet-3413	47	30	multiple	multiple	ADJ
cet-3413	47	31	reaction	reaction	NOUN
cet-3413	47	32	system	system	NOUN
cet-3413	47	33	.	.	PUNCT
cet-3413	48	1	an	an	DET
cet-3413	48	2	example	example	NOUN
cet-3413	48	3	of	of	ADP
cet-3413	48	4	possible	possible	ADJ
cet-3413	48	5	reaction	reaction	NOUN
cet-3413	48	6	mechanisms	mechanism	NOUN
cet-3413	48	7	is	be	AUX
cet-3413	48	8	shown	show	VERB
cet-3413	48	9	in	in	ADP
cet-3413	48	10	figure	figure	NOUN
cet-3413	48	11	5	5	NUM
cet-3413	48	12	(	(	PUNCT
cet-3413	48	13	neuenfeld	neuenfeld	ADJ
cet-3413	48	14	,	,	PUNCT
cet-3413	48	15	2008	2008	NUM
cet-3413	48	16	)	)	PUNCT
cet-3413	48	17	,	,	PUNCT
cet-3413	48	18	which	which	PRON
cet-3413	48	19	are	be	AUX
cet-3413	48	20	followed	follow	VERB
cet-3413	48	21	by	by	ADP
cet-3413	48	22	further	further	ADJ
cet-3413	48	23	decomposition	decomposition	NOUN
cet-3413	48	24	steps	step	NOUN
cet-3413	48	25	.	.	PUNCT
cet-3413	49	1	figure	figure	VERB
cet-3413	49	2	5	5	NUM
cet-3413	49	3	:	:	PUNCT
cet-3413	49	4	possible	possible	ADJ
cet-3413	49	5	reaction	reaction	NOUN
cet-3413	49	6	mechanisms	mechanism	NOUN
cet-3413	49	7	for	for	ADP
cet-3413	49	8	the	the	DET
cet-3413	49	9	reaction	reaction	NOUN
cet-3413	49	10	of	of	ADP
cet-3413	49	11	morpholine	morpholine	NOUN
cet-3413	49	12	and	and	CCONJ
cet-3413	49	13	dichloromethane	dichloromethane	NOUN
cet-3413	49	14	(	(	PUNCT
cet-3413	49	15	neuenfeld	neuenfeld	ADJ
cet-3413	49	16	,	,	PUNCT
cet-3413	49	17	2008	2008	NUM
cet-3413	49	18	)	)	PUNCT
cet-3413	50	1	2	2	NUM
cet-3413	50	2	.	.	PUNCT
cet-3413	50	3	adiabatic	adiabatic	ADJ
cet-3413	50	4	calorimetry	calorimetry	NOUN
cet-3413	50	5	on	on	ADP
cet-3413	50	6	the	the	DET
cet-3413	50	7	basis	basis	NOUN
cet-3413	50	8	of	of	ADP
cet-3413	50	9	the	the	DET
cet-3413	50	10	results	result	NOUN
cet-3413	50	11	of	of	ADP
cet-3413	50	12	the	the	DET
cet-3413	50	13	dsc	dsc	NOUN
cet-3413	50	14	measurements	measurement	NOUN
cet-3413	50	15	,	,	PUNCT
cet-3413	50	16	two	two	NUM
cet-3413	50	17	different	different	ADJ
cet-3413	50	18	amine	amine	ADJ
cet-3413	50	19	compounds	compound	NOUN
cet-3413	50	20	were	be	AUX
cet-3413	50	21	investigated	investigate	VERB
cet-3413	50	22	using	use	VERB
cet-3413	50	23	two	two	NUM
cet-3413	50	24	different	different	ADJ
cet-3413	50	25	adiabatic	adiabatic	ADJ
cet-3413	50	26	calorimetry	calorimetry	NOUN
cet-3413	50	27	techniques	technique	NOUN
cet-3413	50	28	:	:	PUNCT
cet-3413	50	29	dewar	dewar	ADJ
cet-3413	50	30	calorimetry	calorimetry	NOUN
cet-3413	50	31	and	and	CCONJ
cet-3413	50	32	vsp2	vsp2	PROPN
cet-3413	50	33	(	(	PUNCT
cet-3413	50	34	vent	vent	VERB
cet-3413	50	35	sizing	size	VERB
cet-3413	50	36	package	package	NOUN
cet-3413	50	37	)	)	PUNCT
cet-3413	50	38	.	.	PUNCT
cet-3413	51	1	2.1	2.1	NUM
cet-3413	51	2	.	.	PUNCT
cet-3413	51	3	dewar	dewar	ADJ
cet-3413	51	4	calorimetry	calorimetry	NOUN
cet-3413	51	5	of	of	ADP
cet-3413	51	6	dipropylamine	dipropylamine	NOUN
cet-3413	51	7	and	and	CCONJ
cet-3413	51	8	dichloromethane	dichloromethane	NOUN
cet-3413	51	9	for	for	ADP
cet-3413	51	10	the	the	DET
cet-3413	51	11	investigation	investigation	NOUN
cet-3413	51	12	of	of	ADP
cet-3413	51	13	the	the	DET
cet-3413	51	14	reactivity	reactivity	NOUN
cet-3413	51	15	of	of	ADP
cet-3413	51	16	dipropylamine	dipropylamine	NOUN
cet-3413	51	17	toward	toward	ADP
cet-3413	51	18	dichloromethane	dichloromethane	NOUN
cet-3413	51	19	(	(	PUNCT
cet-3413	51	20	ratio	ratio	NOUN
cet-3413	51	21	2:1	2:1	NUM
cet-3413	51	22	)	)	PUNCT
cet-3413	51	23	the	the	DET
cet-3413	51	24	investigation	investigation	NOUN
cet-3413	51	25	was	be	AUX
cet-3413	51	26	performed	perform	VERB
cet-3413	51	27	by	by	ADP
cet-3413	51	28	using	use	VERB
cet-3413	51	29	dewar	dewar	ADJ
cet-3413	51	30	calorimetry	calorimetry	NOUN
cet-3413	51	31	.	.	PUNCT
cet-3413	52	1	for	for	ADP
cet-3413	52	2	this	this	DET
cet-3413	52	3	purpose	purpose	NOUN
cet-3413	52	4	,	,	PUNCT
cet-3413	52	5	about	about	ADV
cet-3413	52	6	95	95	NUM
cet-3413	52	7	g	g	NOUN
cet-3413	52	8	of	of	ADP
cet-3413	52	9	the	the	DET
cet-3413	52	10	mixture	mixture	NOUN
cet-3413	52	11	were	be	AUX
cet-3413	52	12	filled	fill	VERB
cet-3413	52	13	into	into	ADP
cet-3413	52	14	a	a	DET
cet-3413	52	15	dewar	dewar	ADJ
cet-3413	52	16	vessel	vessel	NOUN
cet-3413	52	17	,	,	PUNCT
cet-3413	52	18	which	which	PRON
cet-3413	52	19	was	be	AUX
cet-3413	52	20	placed	place	VERB
cet-3413	52	21	in	in	ADP
cet-3413	52	22	a	a	DET
cet-3413	52	23	high	high	ADJ
cet-3413	52	24	pressure	pressure	NOUN
cet-3413	52	25	autoclave	autoclave	NOUN
cet-3413	52	26	with	with	ADP
cet-3413	52	27	a	a	DET
cet-3413	52	28	volume	volume	NOUN
cet-3413	52	29	of	of	ADP
cet-3413	52	30	0.75	0.75	NUM
cet-3413	52	31	l.	l.	NOUN
cet-3413	52	32	this	this	DET
cet-3413	52	33	autoclave	autoclave	NOUN
cet-3413	52	34	was	be	AUX
cet-3413	52	35	closed	close	VERB
cet-3413	52	36	and	and	CCONJ
cet-3413	52	37	put	put	VERB
cet-3413	52	38	into	into	ADP
cet-3413	52	39	an	an	DET
cet-3413	52	40	aluminium	aluminium	NOUN
cet-3413	52	41	oven	oven	NOUN
cet-3413	52	42	.	.	PUNCT
cet-3413	53	1	the	the	DET
cet-3413	53	2	sample	sample	NOUN
cet-3413	53	3	was	be	AUX
cet-3413	53	4	heated	heat	VERB
cet-3413	53	5	up	up	ADP
cet-3413	53	6	to	to	ADP
cet-3413	53	7	storage	storage	NOUN
cet-3413	53	8	temperature	temperature	NOUN
cet-3413	53	9	of	of	ADP
cet-3413	53	10	55	55	NUM
cet-3413	53	11	°	°	NOUN
cet-3413	53	12	c	c	NOUN
cet-3413	53	13	.	.	PUNCT
cet-3413	54	1	since	since	SCONJ
cet-3413	54	2	no	no	DET
cet-3413	54	3	significant	significant	ADJ
cet-3413	54	4	exothermic	exothermic	ADJ
cet-3413	54	5	effect	effect	NOUN
cet-3413	54	6	was	be	AUX
cet-3413	54	7	observed	observe	VERB
cet-3413	54	8	within	within	ADP
cet-3413	54	9	24	24	NUM
cet-3413	54	10	h	h	NOUN
cet-3413	54	11	,	,	PUNCT
cet-3413	54	12	the	the	DET
cet-3413	54	13	temperature	temperature	NOUN
cet-3413	54	14	was	be	AUX
cet-3413	54	15	increased	increase	VERB
cet-3413	54	16	stepwise	stepwise	NOUN
cet-3413	54	17	until	until	SCONJ
cet-3413	54	18	a	a	DET
cet-3413	54	19	runaway	runaway	ADJ
cet-3413	54	20	reaction	reaction	NOUN
cet-3413	54	21	could	could	AUX
cet-3413	54	22	be	be	AUX
cet-3413	54	23	detected	detect	VERB
cet-3413	54	24	.	.	PUNCT
cet-3413	55	1	during	during	ADP
cet-3413	55	2	the	the	DET
cet-3413	55	3	run	run	NOUN
cet-3413	55	4	away	away	ADV
cet-3413	55	5	reaction	reaction	NOUN
cet-3413	55	6	,	,	PUNCT
cet-3413	55	7	the	the	DET
cet-3413	55	8	temperature	temperature	NOUN
cet-3413	55	9	of	of	ADP
cet-3413	55	10	the	the	DET
cet-3413	55	11	aluminium	aluminium	NOUN
cet-3413	55	12	oven	oven	NOUN
cet-3413	55	13	was	be	AUX
cet-3413	55	14	adjusted	adjust	VERB
cet-3413	55	15	to	to	ADP
cet-3413	55	16	the	the	DET
cet-3413	55	17	temperature	temperature	NOUN
cet-3413	55	18	of	of	ADP
cet-3413	55	19	the	the	DET
cet-3413	55	20	sample	sample	NOUN
cet-3413	55	21	.	.	PUNCT
cet-3413	56	1	the	the	DET
cet-3413	56	2	course	course	NOUN
cet-3413	56	3	of	of	ADP
cet-3413	56	4	the	the	DET
cet-3413	56	5	temperature	temperature	NOUN
cet-3413	56	6	and	and	CCONJ
cet-3413	56	7	pressure	pressure	NOUN
cet-3413	56	8	were	be	AUX
cet-3413	56	9	recorded	record	VERB
cet-3413	56	10	during	during	ADP
cet-3413	56	11	the	the	DET
cet-3413	56	12	whole	whole	ADJ
cet-3413	56	13	test	test	NOUN
cet-3413	56	14	.	.	PUNCT
cet-3413	57	1	figure	figure	NOUN
cet-3413	57	2	6	6	NUM
cet-3413	57	3	shows	show	VERB
cet-3413	57	4	the	the	DET
cet-3413	57	5	course	course	NOUN
cet-3413	57	6	of	of	ADP
cet-3413	57	7	the	the	DET
cet-3413	57	8	temperature	temperature	NOUN
cet-3413	57	9	and	and	CCONJ
cet-3413	57	10	pressure	pressure	NOUN
cet-3413	57	11	during	during	ADP
cet-3413	57	12	the	the	DET
cet-3413	57	13	test	test	NOUN
cet-3413	57	14	.	.	PUNCT
cet-3413	58	1	an	an	DET
cet-3413	58	2	exothermic	exothermic	ADJ
cet-3413	58	3	reaction	reaction	NOUN
cet-3413	58	4	was	be	AUX
cet-3413	58	5	detected	detect	VERB
cet-3413	58	6	starting	start	VERB
cet-3413	58	7	at	at	ADP
cet-3413	58	8	a	a	DET
cet-3413	58	9	temperature	temperature	NOUN
cet-3413	58	10	of	of	ADP
cet-3413	58	11	about	about	ADV
cet-3413	58	12	70	70	NUM
cet-3413	58	13	°	°	NOUN
cet-3413	58	14	c	c	NOUN
cet-3413	58	15	.	.	PUNCT
cet-3413	59	1	the	the	DET
cet-3413	59	2	reaction	reaction	NOUN
cet-3413	59	3	reaches	reach	VERB
cet-3413	59	4	a	a	DET
cet-3413	59	5	maximum	maximum	ADJ
cet-3413	59	6	temperature	temperature	NOUN
cet-3413	59	7	of	of	ADP
cet-3413	59	8	216	216	NUM
cet-3413	59	9	°	°	NOUN
cet-3413	59	10	c	c	NOUN
cet-3413	59	11	after	after	ADP
cet-3413	59	12	170	170	NUM
cet-3413	59	13	hours	hour	NOUN
cet-3413	59	14	.	.	PUNCT
cet-3413	60	1	figure	figure	VERB
cet-3413	60	2	6	6	NUM
cet-3413	60	3	:	:	PUNCT
cet-3413	60	4	temperature	temperature	NOUN
cet-3413	60	5	and	and	CCONJ
cet-3413	60	6	pressure	pressure	NOUN
cet-3413	60	7	course	course	NOUN
cet-3413	60	8	of	of	ADP
cet-3413	60	9	dipropylamine	dipropylamine	NOUN
cet-3413	60	10	and	and	CCONJ
cet-3413	60	11	dichloromethane	dichloromethane	NOUN
cet-3413	60	12	(	(	PUNCT
cet-3413	60	13	ratio	ratio	NOUN
cet-3413	60	14	2:1	2:1	NUM
cet-3413	60	15	)	)	PUNCT
cet-3413	61	1	766	766	NUM
cet-3413	61	2	figure	figure	NOUN
cet-3413	61	3	7	7	NUM
cet-3413	61	4	:	:	PUNCT
cet-3413	61	5	temperature	temperature	NOUN
cet-3413	61	6	and	and	CCONJ
cet-3413	61	7	pressure	pressure	NOUN
cet-3413	61	8	increase	increase	NOUN
cet-3413	61	9	rate	rate	NOUN
cet-3413	61	10	of	of	ADP
cet-3413	61	11	dipropylamine	dipropylamine	NOUN
cet-3413	61	12	and	and	CCONJ
cet-3413	61	13	dichloromethane	dichloromethane	NOUN
cet-3413	61	14	(	(	PUNCT
cet-3413	61	15	ratio	ratio	NOUN
cet-3413	61	16	2:1	2:1	NUM
cet-3413	61	17	)	)	PUNCT
cet-3413	61	18	the	the	DET
cet-3413	61	19	pressure	pressure	NOUN
cet-3413	61	20	increase	increase	VERB
cet-3413	61	21	the	the	DET
cet-3413	61	22	pressure	pressure	NOUN
cet-3413	61	23	increase	increase	NOUN
cet-3413	61	24	rate	rate	NOUN
cet-3413	61	25	shown	show	VERB
cet-3413	61	26	in	in	ADP
cet-3413	61	27	figure	figure	NOUN
cet-3413	61	28	7	7	NUM
cet-3413	61	29	can	can	AUX
cet-3413	61	30	be	be	AUX
cet-3413	61	31	derived	derive	VERB
cet-3413	61	32	from	from	ADP
cet-3413	61	33	the	the	DET
cet-3413	61	34	first	first	ADJ
cet-3413	61	35	derivative	derivative	NOUN
cet-3413	61	36	of	of	ADP
cet-3413	61	37	the	the	DET
cet-3413	61	38	time	time	NOUN
cet-3413	61	39	resolved	resolve	VERB
cet-3413	61	40	course	course	NOUN
cet-3413	61	41	of	of	ADP
cet-3413	61	42	t.	t.	NOUN
cet-3413	61	43	this	this	DET
cet-3413	61	44	rate	rate	NOUN
cet-3413	61	45	includes	include	VERB
cet-3413	61	46	the	the	DET
cet-3413	61	47	pressure	pressure	NOUN
cet-3413	61	48	increase	increase	NOUN
cet-3413	61	49	caused	cause	VERB
cet-3413	61	50	by	by	ADP
cet-3413	61	51	other	other	ADJ
cet-3413	61	52	effects	effect	NOUN
cet-3413	61	53	,	,	PUNCT
cet-3413	61	54	like	like	ADP
cet-3413	61	55	vapour	vapour	NOUN
cet-3413	61	56	pressure	pressure	NOUN
cet-3413	61	57	increase	increase	NOUN
cet-3413	61	58	and	and	CCONJ
cet-3413	61	59	thermal	thermal	ADJ
cet-3413	61	60	expansion	expansion	NOUN
cet-3413	61	61	of	of	ADP
cet-3413	61	62	the	the	DET
cet-3413	61	63	liquid	liquid	NOUN
cet-3413	61	64	.	.	PUNCT
cet-3413	62	1	the	the	DET
cet-3413	62	2	maximum	maximum	ADJ
cet-3413	62	3	pressure	pressure	NOUN
cet-3413	62	4	increase	increase	NOUN
cet-3413	62	5	rate	rate	NOUN
cet-3413	62	6	of	of	ADP
cet-3413	62	7	the	the	DET
cet-3413	62	8	mixture	mixture	NOUN
cet-3413	62	9	of	of	ADP
cet-3413	62	10	about	about	ADV
cet-3413	62	11	0.2	0.2	NUM
cet-3413	62	12	bar	bar	NOUN
cet-3413	62	13	/	/	SYM
cet-3413	62	14	min	min	NOUN
cet-3413	62	15	was	be	AUX
cet-3413	62	16	observed	observe	VERB
cet-3413	62	17	in	in	ADP
cet-3413	62	18	the	the	DET
cet-3413	62	19	temperature	temperature	NOUN
cet-3413	62	20	range	range	NOUN
cet-3413	62	21	from	from	ADP
cet-3413	62	22	165	165	NUM
cet-3413	62	23	to	to	PART
cet-3413	62	24	180	180	NUM
cet-3413	62	25	°	°	NOUN
cet-3413	62	26	c	c	NOUN
cet-3413	62	27	.	.	PUNCT
cet-3413	63	1	from	from	ADP
cet-3413	63	2	the	the	DET
cet-3413	63	3	course	course	NOUN
cet-3413	63	4	of	of	ADP
cet-3413	63	5	the	the	DET
cet-3413	63	6	temperature	temperature	NOUN
cet-3413	63	7	trace	trace	NOUN
cet-3413	63	8	,	,	PUNCT
cet-3413	63	9	the	the	DET
cet-3413	63	10	temperature	temperature	NOUN
cet-3413	63	11	increase	increase	NOUN
cet-3413	63	12	rate	rate	NOUN
cet-3413	63	13	can	can	AUX
cet-3413	63	14	be	be	AUX
cet-3413	63	15	derived	derive	VERB
cet-3413	63	16	,	,	PUNCT
cet-3413	63	17	which	which	PRON
cet-3413	63	18	is	be	AUX
cet-3413	63	19	also	also	ADV
cet-3413	63	20	shown	show	VERB
cet-3413	63	21	in	in	ADP
cet-3413	63	22	figure	figure	NOUN
cet-3413	63	23	4	4	NUM
cet-3413	63	24	.	.	PUNCT
cet-3413	64	1	the	the	DET
cet-3413	64	2	temperature	temperature	NOUN
cet-3413	64	3	rise	rise	NOUN
cet-3413	64	4	rate	rate	NOUN
cet-3413	64	5	reaches	reach	VERB
cet-3413	64	6	its	its	PRON
cet-3413	64	7	maximum	maximum	NOUN
cet-3413	64	8	of	of	ADP
cet-3413	64	9	8	8	NUM
cet-3413	64	10	k	k	NOUN
cet-3413	64	11	/	/	SYM
cet-3413	64	12	min	min	NOUN
cet-3413	64	13	at	at	ADP
cet-3413	64	14	temperature	temperature	NOUN
cet-3413	64	15	of	of	ADP
cet-3413	64	16	about	about	ADV
cet-3413	64	17	210	210	NUM
cet-3413	64	18	°	°	NOUN
cet-3413	64	19	c	c	NOUN
cet-3413	64	20	.	.	PUNCT
cet-3413	65	1	2.2	2.2	NUM
cet-3413	65	2	.	.	PUNCT
cet-3413	65	3	adiabatic	adiabatic	ADJ
cet-3413	65	4	test	test	NOUN
cet-3413	65	5	with	with	ADP
cet-3413	65	6	the	the	DET
cet-3413	65	7	vsp2	vsp2	NOUN
cet-3413	65	8	with	with	ADP
cet-3413	65	9	piperidine	piperidine	NOUN
cet-3413	65	10	and	and	CCONJ
cet-3413	65	11	dichloromethane	dichloromethane	NOUN
cet-3413	65	12	for	for	ADP
cet-3413	65	13	the	the	DET
cet-3413	65	14	investigation	investigation	NOUN
cet-3413	65	15	of	of	ADP
cet-3413	65	16	the	the	DET
cet-3413	65	17	reactivity	reactivity	NOUN
cet-3413	65	18	of	of	ADP
cet-3413	65	19	piperidine	piperidine	NOUN
cet-3413	65	20	toward	toward	ADP
cet-3413	65	21	dichloromethane	dichloromethane	NOUN
cet-3413	65	22	(	(	PUNCT
cet-3413	65	23	ratio	ratio	NOUN
cet-3413	65	24	2:1	2:1	NUM
cet-3413	65	25	)	)	PUNCT
cet-3413	65	26	,	,	PUNCT
cet-3413	65	27	the	the	DET
cet-3413	65	28	investigation	investigation	NOUN
cet-3413	65	29	was	be	AUX
cet-3413	65	30	performed	perform	VERB
cet-3413	65	31	using	use	VERB
cet-3413	65	32	the	the	DET
cet-3413	65	33	adiabatic	adiabatic	ADJ
cet-3413	65	34	calorimeter	calorimeter	NOUN
cet-3413	65	35	vsp2	vsp2	NOUN
cet-3413	65	36	(	(	PUNCT
cet-3413	65	37	fauske	fauske	PROPN
cet-3413	65	38	&	&	CCONJ
cet-3413	65	39	associates	associates	PROPN
cet-3413	65	40	,	,	PUNCT
cet-3413	65	41	llc	llc	PROPN
cet-3413	65	42	)	)	PUNCT
cet-3413	65	43	.	.	PUNCT
cet-3413	66	1	for	for	ADP
cet-3413	66	2	this	this	DET
cet-3413	66	3	purpose	purpose	NOUN
cet-3413	66	4	,	,	PUNCT
cet-3413	66	5	about	about	ADV
cet-3413	66	6	35	35	NUM
cet-3413	66	7	g	g	NOUN
cet-3413	66	8	of	of	ADP
cet-3413	66	9	the	the	DET
cet-3413	66	10	mixture	mixture	NOUN
cet-3413	66	11	were	be	AUX
cet-3413	66	12	filled	fill	VERB
cet-3413	66	13	into	into	ADP
cet-3413	66	14	a	a	DET
cet-3413	66	15	thin	thin	ADJ
cet-3413	66	16	walled	walled	ADJ
cet-3413	66	17	steel	steel	NOUN
cet-3413	66	18	test	test	NOUN
cet-3413	66	19	cell	cell	NOUN
cet-3413	66	20	with	with	ADP
cet-3413	66	21	a	a	DET
cet-3413	66	22	volume	volume	NOUN
cet-3413	66	23	of	of	ADP
cet-3413	66	24	110	110	NUM
cet-3413	66	25	ml	ml	NOUN
cet-3413	66	26	.	.	PUNCT
cet-3413	67	1	the	the	DET
cet-3413	67	2	test	test	NOUN
cet-3413	67	3	cell	cell	NOUN
cet-3413	67	4	was	be	AUX
cet-3413	67	5	placed	place	VERB
cet-3413	67	6	into	into	ADP
cet-3413	67	7	a	a	DET
cet-3413	67	8	heater	heater	NOUN
cet-3413	67	9	assembly	assembly	NOUN
cet-3413	67	10	,	,	PUNCT
cet-3413	67	11	which	which	PRON
cet-3413	67	12	was	be	AUX
cet-3413	67	13	installed	instal	VERB
cet-3413	67	14	into	into	ADP
cet-3413	67	15	4	4	NUM
cet-3413	67	16	l	l	NOUN
cet-3413	67	17	pressure	pressure	NOUN
cet-3413	67	18	vessel	vessel	NOUN
cet-3413	67	19	.	.	PUNCT
cet-3413	68	1	the	the	DET
cet-3413	68	2	pressure	pressure	NOUN
cet-3413	68	3	vessel	vessel	NOUN
cet-3413	68	4	was	be	AUX
cet-3413	68	5	closed	close	VERB
cet-3413	68	6	and	and	CCONJ
cet-3413	68	7	the	the	DET
cet-3413	68	8	test	test	NOUN
cet-3413	68	9	was	be	AUX
cet-3413	68	10	started	start	VERB
cet-3413	68	11	at	at	ADP
cet-3413	68	12	ambient	ambient	ADJ
cet-3413	68	13	temperature	temperature	NOUN
cet-3413	68	14	.	.	PUNCT
cet-3413	69	1	a	a	DET
cet-3413	69	2	slow	slow	ADJ
cet-3413	69	3	exothermic	exothermic	ADJ
cet-3413	69	4	reaction	reaction	NOUN
cet-3413	69	5	was	be	AUX
cet-3413	69	6	detected	detect	VERB
cet-3413	69	7	at	at	ADP
cet-3413	69	8	ambient	ambient	ADJ
cet-3413	69	9	temperature	temperature	NOUN
cet-3413	69	10	and	and	CCONJ
cet-3413	69	11	the	the	DET
cet-3413	69	12	sample	sample	NOUN
cet-3413	69	13	temperature	temperature	NOUN
cet-3413	69	14	was	be	AUX
cet-3413	69	15	followed	follow	VERB
cet-3413	69	16	by	by	ADP
cet-3413	69	17	the	the	DET
cet-3413	69	18	heater	heater	NOUN
cet-3413	69	19	of	of	ADP
cet-3413	69	20	the	the	DET
cet-3413	69	21	vsp2	vsp2	PROPN
cet-3413	69	22	.	.	PUNCT
cet-3413	70	1	the	the	DET
cet-3413	70	2	temperature	temperature	NOUN
cet-3413	70	3	increase	increase	NOUN
cet-3413	70	4	led	lead	VERB
cet-3413	70	5	to	to	ADP
cet-3413	70	6	a	a	DET
cet-3413	70	7	runaway	runaway	ADJ
cet-3413	70	8	reaction	reaction	NOUN
cet-3413	70	9	within	within	ADP
cet-3413	70	10	a	a	DET
cet-3413	70	11	time	time	NOUN
cet-3413	70	12	period	period	NOUN
cet-3413	70	13	of	of	ADP
cet-3413	70	14	about	about	ADV
cet-3413	70	15	210	210	NUM
cet-3413	70	16	min	min	NOUN
cet-3413	70	17	.	.	PROPN
cet-3413	70	18	to	to	PART
cet-3413	70	19	avoid	avoid	VERB
cet-3413	70	20	a	a	DET
cet-3413	70	21	bursting	bursting	NOUN
cet-3413	70	22	of	of	ADP
cet-3413	70	23	the	the	DET
cet-3413	70	24	test	test	NOUN
cet-3413	70	25	cell	cell	NOUN
cet-3413	70	26	due	due	ADP
cet-3413	70	27	to	to	ADP
cet-3413	70	28	pressure	pressure	NOUN
cet-3413	70	29	increase	increase	NOUN
cet-3413	70	30	inside	inside	ADP
cet-3413	70	31	the	the	DET
cet-3413	70	32	test	test	NOUN
cet-3413	70	33	cell	cell	NOUN
cet-3413	70	34	,	,	PUNCT
cet-3413	70	35	the	the	DET
cet-3413	70	36	pressure	pressure	NOUN
cet-3413	70	37	inside	inside	ADP
cet-3413	70	38	the	the	DET
cet-3413	70	39	4	4	NUM
cet-3413	70	40	l	l	NOUN
cet-3413	70	41	pressure	pressure	NOUN
cet-3413	70	42	vessel	vessel	NOUN
cet-3413	70	43	was	be	AUX
cet-3413	70	44	adjusted	adjust	VERB
cet-3413	70	45	slightly	slightly	ADV
cet-3413	70	46	below	below	ADP
cet-3413	70	47	the	the	DET
cet-3413	70	48	pressure	pressure	NOUN
cet-3413	70	49	of	of	ADP
cet-3413	70	50	the	the	DET
cet-3413	70	51	test	test	NOUN
cet-3413	70	52	cell	cell	NOUN
cet-3413	70	53	.	.	PUNCT
cet-3413	71	1	the	the	DET
cet-3413	71	2	course	course	NOUN
cet-3413	71	3	of	of	ADP
cet-3413	71	4	the	the	DET
cet-3413	71	5	temperature	temperature	NOUN
cet-3413	71	6	and	and	CCONJ
cet-3413	71	7	pressure	pressure	NOUN
cet-3413	71	8	were	be	AUX
cet-3413	71	9	recorded	record	VERB
cet-3413	71	10	during	during	ADP
cet-3413	71	11	the	the	DET
cet-3413	71	12	whole	whole	ADJ
cet-3413	71	13	test	test	NOUN
cet-3413	71	14	.	.	PUNCT
cet-3413	72	1	figure	figure	VERB
cet-3413	72	2	8	8	NUM
cet-3413	72	3	:	:	PUNCT
cet-3413	72	4	temperature	temperature	NOUN
cet-3413	72	5	and	and	CCONJ
cet-3413	72	6	pressure	pressure	NOUN
cet-3413	72	7	course	course	NOUN
cet-3413	72	8	of	of	ADP
cet-3413	72	9	piperidine	piperidine	NOUN
cet-3413	72	10	and	and	CCONJ
cet-3413	72	11	dichloromethane	dichloromethane	NOUN
cet-3413	72	12	(	(	PUNCT
cet-3413	72	13	ratio	ratio	NOUN
cet-3413	72	14	2:1	2:1	NUM
cet-3413	72	15	)	)	PUNCT
cet-3413	72	16	767	767	NUM
cet-3413	72	17	figure	figure	NOUN
cet-3413	72	18	8	8	NUM
cet-3413	72	19	shows	show	VERB
cet-3413	72	20	the	the	DET
cet-3413	72	21	course	course	NOUN
cet-3413	72	22	of	of	ADP
cet-3413	72	23	the	the	DET
cet-3413	72	24	temperature	temperature	NOUN
cet-3413	72	25	and	and	CCONJ
cet-3413	72	26	pressure	pressure	NOUN
cet-3413	72	27	during	during	ADP
cet-3413	72	28	the	the	DET
cet-3413	72	29	test	test	NOUN
cet-3413	72	30	.	.	PUNCT
cet-3413	73	1	the	the	DET
cet-3413	73	2	reaction	reaction	NOUN
cet-3413	73	3	starts	start	VERB
cet-3413	73	4	at	at	ADP
cet-3413	73	5	ambient	ambient	ADJ
cet-3413	73	6	temperature	temperature	NOUN
cet-3413	73	7	reaching	reach	VERB
cet-3413	73	8	a	a	DET
cet-3413	73	9	maximum	maximum	ADJ
cet-3413	73	10	reaction	reaction	NOUN
cet-3413	73	11	temperature	temperature	NOUN
cet-3413	73	12	of	of	ADP
cet-3413	73	13	400	400	NUM
cet-3413	73	14	°	°	NOUN
cet-3413	73	15	c	c	NOUN
cet-3413	73	16	after	after	ADP
cet-3413	73	17	a	a	DET
cet-3413	73	18	time	time	NOUN
cet-3413	73	19	period	period	NOUN
cet-3413	73	20	of	of	ADP
cet-3413	73	21	213	213	NUM
cet-3413	73	22	min	min	NOUN
cet-3413	73	23	.	.	PROPN
cet-3413	74	1	a	a	DET
cet-3413	74	2	maximum	maximum	ADJ
cet-3413	74	3	pressure	pressure	NOUN
cet-3413	74	4	of	of	ADP
cet-3413	74	5	53	53	NUM
cet-3413	74	6	barg	barg	NOUN
cet-3413	74	7	was	be	AUX
cet-3413	74	8	detected	detect	VERB
cet-3413	74	9	at	at	ADP
cet-3413	74	10	this	this	DET
cet-3413	74	11	point	point	NOUN
cet-3413	74	12	.	.	PUNCT
cet-3413	75	1	using	use	VERB
cet-3413	75	2	a	a	DET
cet-3413	75	3	thermal	thermal	ADJ
cet-3413	75	4	inertia	inertia	NOUN
cet-3413	75	5	of	of	ADP
cet-3413	75	6	ᵠ=1.3	ᵠ=1.3	PROPN
cet-3413	75	7	and	and	CCONJ
cet-3413	75	8	the	the	DET
cet-3413	75	9	observed	observe	VERB
cet-3413	75	10	temperature	temperature	NOUN
cet-3413	75	11	increase	increase	NOUN
cet-3413	75	12	of	of	ADP
cet-3413	75	13	374	374	NUM
cet-3413	75	14	k	k	NOUN
cet-3413	75	15	(	(	PUNCT
cet-3413	75	16	temperature	temperature	NOUN
cet-3413	75	17	increase	increase	NOUN
cet-3413	75	18	from	from	ADP
cet-3413	75	19	27	27	NUM
cet-3413	75	20	°	°	NOUN
cet-3413	75	21	c	c	NOUN
cet-3413	75	22	to	to	ADP
cet-3413	75	23	401	401	NUM
cet-3413	75	24	°	°	NOUN
cet-3413	75	25	c	c	NOUN
cet-3413	75	26	)	)	PUNCT
cet-3413	75	27	an	an	DET
cet-3413	75	28	adiabatic	adiabatic	ADJ
cet-3413	75	29	temperature	temperature	NOUN
cet-3413	75	30	rise	rise	NOUN
cet-3413	75	31	of	of	ADP
cet-3413	75	32	∆tad	∆tad	NOUN
cet-3413	75	33	=	=	SYM
cet-3413	75	34	490	490	NUM
cet-3413	75	35	k	k	NOUN
cet-3413	75	36	was	be	AUX
cet-3413	75	37	observed	observe	VERB
cet-3413	75	38	.	.	PUNCT
cet-3413	76	1	figure	figure	VERB
cet-3413	76	2	9	9	NUM
cet-3413	76	3	:	:	PUNCT
cet-3413	76	4	temperature	temperature	NOUN
cet-3413	76	5	and	and	CCONJ
cet-3413	76	6	pressure	pressure	NOUN
cet-3413	76	7	increase	increase	NOUN
cet-3413	76	8	rate	rate	NOUN
cet-3413	76	9	of	of	ADP
cet-3413	76	10	piperidine	piperidine	NOUN
cet-3413	76	11	and	and	CCONJ
cet-3413	76	12	dichloromethane	dichloromethane	NOUN
cet-3413	76	13	(	(	PUNCT
cet-3413	76	14	ratio	ratio	NOUN
cet-3413	76	15	2:1	2:1	NUM
cet-3413	76	16	)	)	PUNCT
cet-3413	76	17	the	the	DET
cet-3413	76	18	pressure	pressure	NOUN
cet-3413	76	19	increase	increase	NOUN
cet-3413	76	20	rate	rate	NOUN
cet-3413	76	21	shown	show	VERB
cet-3413	76	22	in	in	ADP
cet-3413	76	23	figure	figure	NOUN
cet-3413	76	24	9	9	NUM
cet-3413	76	25	can	can	AUX
cet-3413	76	26	be	be	AUX
cet-3413	76	27	derived	derive	VERB
cet-3413	76	28	from	from	ADP
cet-3413	76	29	the	the	DET
cet-3413	76	30	first	first	ADJ
cet-3413	76	31	derivative	derivative	NOUN
cet-3413	76	32	of	of	ADP
cet-3413	76	33	the	the	DET
cet-3413	76	34	time	time	NOUN
cet-3413	76	35	resolved	resolve	VERB
cet-3413	76	36	course	course	NOUN
cet-3413	76	37	of	of	ADP
cet-3413	76	38	the	the	DET
cet-3413	76	39	pressure	pressure	NOUN
cet-3413	76	40	increase	increase	NOUN
cet-3413	76	41	.	.	PUNCT
cet-3413	77	1	this	this	DET
cet-3413	77	2	rate	rate	NOUN
cet-3413	77	3	includes	include	VERB
cet-3413	77	4	the	the	DET
cet-3413	77	5	pressure	pressure	NOUN
cet-3413	77	6	increase	increase	NOUN
cet-3413	77	7	caused	cause	VERB
cet-3413	77	8	by	by	ADP
cet-3413	77	9	other	other	ADJ
cet-3413	77	10	effects	effect	NOUN
cet-3413	77	11	,	,	PUNCT
cet-3413	77	12	like	like	ADP
cet-3413	77	13	vapour	vapour	NOUN
cet-3413	77	14	pressure	pressure	NOUN
cet-3413	77	15	increase	increase	NOUN
cet-3413	77	16	and	and	CCONJ
cet-3413	77	17	thermal	thermal	ADJ
cet-3413	77	18	expansion	expansion	NOUN
cet-3413	77	19	of	of	ADP
cet-3413	77	20	the	the	DET
cet-3413	77	21	liquid	liquid	NOUN
cet-3413	77	22	.	.	PUNCT
cet-3413	78	1	the	the	DET
cet-3413	78	2	maximum	maximum	ADJ
cet-3413	78	3	pressure	pressure	NOUN
cet-3413	78	4	increase	increase	NOUN
cet-3413	78	5	rate	rate	NOUN
cet-3413	78	6	of	of	ADP
cet-3413	78	7	the	the	DET
cet-3413	78	8	mixture	mixture	NOUN
cet-3413	78	9	of	of	ADP
cet-3413	78	10	about	about	ADV
cet-3413	78	11	400	400	NUM
cet-3413	78	12	bar	bar	NOUN
cet-3413	78	13	/	/	SYM
cet-3413	78	14	min	min	NOUN
cet-3413	78	15	was	be	AUX
cet-3413	78	16	observed	observe	VERB
cet-3413	78	17	in	in	ADP
cet-3413	78	18	the	the	DET
cet-3413	78	19	temperature	temperature	NOUN
cet-3413	78	20	range	range	NOUN
cet-3413	78	21	from	from	ADP
cet-3413	78	22	350	350	NUM
cet-3413	78	23	to	to	PART
cet-3413	78	24	370	370	NUM
cet-3413	78	25	°	°	NOUN
cet-3413	78	26	c	c	NOUN
cet-3413	78	27	.	.	PUNCT
cet-3413	79	1	from	from	ADP
cet-3413	79	2	the	the	DET
cet-3413	79	3	course	course	NOUN
cet-3413	79	4	of	of	ADP
cet-3413	79	5	the	the	DET
cet-3413	79	6	temperature	temperature	NOUN
cet-3413	79	7	trace	trace	NOUN
cet-3413	79	8	,	,	PUNCT
cet-3413	79	9	the	the	DET
cet-3413	79	10	temperature	temperature	NOUN
cet-3413	79	11	increase	increase	NOUN
cet-3413	79	12	rate	rate	NOUN
cet-3413	79	13	can	can	AUX
cet-3413	79	14	be	be	AUX
cet-3413	79	15	derived	derive	VERB
cet-3413	79	16	.	.	PUNCT
cet-3413	80	1	the	the	DET
cet-3413	80	2	maximum	maximum	ADJ
cet-3413	80	3	temperature	temperature	NOUN
cet-3413	80	4	increase	increase	NOUN
cet-3413	80	5	rate	rate	NOUN
cet-3413	80	6	was	be	AUX
cet-3413	80	7	found	find	VERB
cet-3413	80	8	to	to	PART
cet-3413	80	9	be	be	AUX
cet-3413	80	10	3300	3300	NUM
cet-3413	80	11	k	k	NOUN
cet-3413	80	12	/	/	SYM
cet-3413	80	13	min	min	NOUN
cet-3413	80	14	observed	observe	VERB
cet-3413	80	15	at	at	ADP
cet-3413	80	16	a	a	DET
cet-3413	80	17	temperature	temperature	NOUN
cet-3413	80	18	of	of	ADP
cet-3413	80	19	approx	approx	NOUN
cet-3413	80	20	.	.	PUNCT
cet-3413	81	1	365	365	NUM
cet-3413	81	2	°	°	NOUN
cet-3413	81	3	c	c	VERB
cet-3413	81	4	.	.	PUNCT
cet-3413	82	1	after	after	ADP
cet-3413	82	2	the	the	DET
cet-3413	82	3	test	test	NOUN
cet-3413	82	4	and	and	CCONJ
cet-3413	82	5	cooling	cool	VERB
cet-3413	82	6	down	down	ADP
cet-3413	82	7	to	to	ADP
cet-3413	82	8	approx	approx	PROPN
cet-3413	82	9	.	.	PUNCT
cet-3413	83	1	20	20	NUM
cet-3413	83	2	°	°	NUM
cet-3413	83	3	c	c	NOUN
cet-3413	83	4	,	,	PUNCT
cet-3413	83	5	the	the	DET
cet-3413	83	6	residual	residual	ADJ
cet-3413	83	7	pressure	pressure	NOUN
cet-3413	83	8	in	in	ADP
cet-3413	83	9	the	the	DET
cet-3413	83	10	autoclave	autoclave	NOUN
cet-3413	83	11	was	be	AUX
cet-3413	83	12	about	about	ADV
cet-3413	83	13	14,5	14,5	NUM
cet-3413	83	14	barg	barg	NOUN
cet-3413	83	15	,	,	PUNCT
cet-3413	83	16	which	which	PRON
cet-3413	83	17	is	be	AUX
cet-3413	83	18	caused	cause	VERB
cet-3413	83	19	by	by	ADP
cet-3413	83	20	the	the	DET
cet-3413	83	21	formation	formation	NOUN
cet-3413	83	22	of	of	ADP
cet-3413	83	23	a	a	DET
cet-3413	83	24	permanent	permanent	ADJ
cet-3413	83	25	,	,	PUNCT
cet-3413	83	26	gaseous	gaseous	ADJ
cet-3413	83	27	compound	compound	NOUN
cet-3413	83	28	.	.	PUNCT
cet-3413	84	1	3	3	X
cet-3413	84	2	.	.	X
cet-3413	84	3	conclusions	conclusion	NOUN
cet-3413	84	4	the	the	DET
cet-3413	84	5	investigations	investigation	NOUN
cet-3413	84	6	via	via	ADP
cet-3413	84	7	dsc	dsc	NOUN
cet-3413	84	8	and	and	CCONJ
cet-3413	84	9	other	other	ADJ
cet-3413	84	10	adiabatic	adiabatic	ADJ
cet-3413	84	11	calorimetric	calorimetric	ADJ
cet-3413	84	12	techniques	technique	NOUN
cet-3413	84	13	of	of	ADP
cet-3413	84	14	the	the	DET
cet-3413	84	15	reaction	reaction	NOUN
cet-3413	84	16	behaviour	behaviour	NOUN
cet-3413	84	17	of	of	ADP
cet-3413	84	18	different	different	ADJ
cet-3413	84	19	amine	amine	ADJ
cet-3413	84	20	compounds	compound	NOUN
cet-3413	84	21	with	with	ADP
cet-3413	84	22	dichloromethane	dichloromethane	NOUN
cet-3413	84	23	show	show	VERB
cet-3413	84	24	a	a	DET
cet-3413	84	25	great	great	ADJ
cet-3413	84	26	reaction	reaction	NOUN
cet-3413	84	27	potential	potential	NOUN
cet-3413	84	28	for	for	ADP
cet-3413	84	29	some	some	DET
cet-3413	84	30	mixtures	mixture	NOUN
cet-3413	84	31	.	.	PUNCT
cet-3413	85	1	for	for	ADP
cet-3413	85	2	aliphaticaromatic	aliphaticaromatic	ADJ
cet-3413	85	3	amines	amine	NOUN
cet-3413	85	4	,	,	PUNCT
cet-3413	85	5	the	the	DET
cet-3413	85	6	decomposition	decomposition	NOUN
cet-3413	85	7	energy	energy	NOUN
cet-3413	85	8	decreases	decrease	VERB
cet-3413	85	9	with	with	ADP
cet-3413	85	10	the	the	DET
cet-3413	85	11	molecular	molecular	ADJ
cet-3413	85	12	weight	weight	NOUN
cet-3413	85	13	of	of	ADP
cet-3413	85	14	the	the	DET
cet-3413	85	15	compound	compound	NOUN
cet-3413	85	16	.	.	PUNCT
cet-3413	86	1	cyclic	cyclic	ADJ
cet-3413	86	2	amines	amine	NOUN
cet-3413	86	3	show	show	VERB
cet-3413	86	4	the	the	DET
cet-3413	86	5	highest	high	ADJ
cet-3413	86	6	decomposition	decomposition	NOUN
cet-3413	86	7	energy	energy	NOUN
cet-3413	86	8	,	,	PUNCT
cet-3413	86	9	which	which	PRON
cet-3413	86	10	is	be	AUX
cet-3413	86	11	also	also	ADV
cet-3413	86	12	accompanied	accompany	VERB
cet-3413	86	13	by	by	ADP
cet-3413	86	14	the	the	DET
cet-3413	86	15	lowest	low	ADJ
cet-3413	86	16	onset	onset	ADJ
cet-3413	86	17	temperatures	temperature	NOUN
cet-3413	86	18	.	.	PUNCT
cet-3413	87	1	in	in	ADP
cet-3413	87	2	addition	addition	NOUN
cet-3413	87	3	,	,	PUNCT
cet-3413	87	4	it	it	PRON
cet-3413	87	5	was	be	AUX
cet-3413	87	6	proven	prove	VERB
cet-3413	87	7	that	that	SCONJ
cet-3413	87	8	the	the	DET
cet-3413	87	9	reactivity	reactivity	NOUN
cet-3413	87	10	decreases	decrease	VERB
cet-3413	87	11	with	with	ADP
cet-3413	87	12	the	the	DET
cet-3413	87	13	number	number	NOUN
cet-3413	87	14	of	of	ADP
cet-3413	87	15	substitutions	substitution	NOUN
cet-3413	87	16	of	of	ADP
cet-3413	87	17	the	the	DET
cet-3413	87	18	amine	amine	ADJ
cet-3413	87	19	compounds	compound	NOUN
cet-3413	87	20	.	.	PUNCT
cet-3413	88	1	in	in	ADP
cet-3413	88	2	the	the	DET
cet-3413	88	3	adiabatic	adiabatic	ADJ
cet-3413	88	4	tests	test	NOUN
cet-3413	88	5	,	,	PUNCT
cet-3413	88	6	a	a	DET
cet-3413	88	7	hazardous	hazardous	ADJ
cet-3413	88	8	reaction	reaction	NOUN
cet-3413	88	9	behaviour	behaviour	NOUN
cet-3413	88	10	in	in	ADP
cet-3413	88	11	regards	regard	NOUN
cet-3413	88	12	of	of	ADP
cet-3413	88	13	the	the	DET
cet-3413	88	14	onset	onset	NOUN
cet-3413	88	15	temperatures	temperature	NOUN
cet-3413	88	16	and	and	CCONJ
cet-3413	88	17	the	the	DET
cet-3413	88	18	temperature	temperature	NOUN
cet-3413	88	19	/	/	SYM
cet-3413	88	20	pressure	pressure	NOUN
cet-3413	88	21	rise	rise	NOUN
cet-3413	88	22	rates	rate	NOUN
cet-3413	88	23	was	be	AUX
cet-3413	88	24	observed	observe	VERB
cet-3413	88	25	.	.	PUNCT
cet-3413	89	1	this	this	PRON
cet-3413	89	2	should	should	AUX
cet-3413	89	3	be	be	AUX
cet-3413	89	4	considered	consider	VERB
cet-3413	89	5	while	while	SCONJ
cet-3413	89	6	handling	handle	VERB
cet-3413	89	7	and	and	CCONJ
cet-3413	89	8	storing	store	VERB
cet-3413	89	9	amine	amine	ADJ
cet-3413	89	10	compounds	compound	NOUN
cet-3413	89	11	diluted	dilute	VERB
cet-3413	89	12	in	in	ADP
cet-3413	89	13	dichloromethane	dichloromethane	NOUN
cet-3413	89	14	in	in	ADP
cet-3413	89	15	closed	closed	ADJ
cet-3413	89	16	systems	system	NOUN
cet-3413	89	17	.	.	PUNCT
cet-3413	90	1	there	there	PRON
cet-3413	90	2	is	be	VERB
cet-3413	90	3	a	a	DET
cet-3413	90	4	great	great	ADJ
cet-3413	90	5	risk	risk	NOUN
cet-3413	90	6	of	of	ADP
cet-3413	90	7	over	over	ADP
cet-3413	90	8	-	-	PUNCT
cet-3413	90	9	pressurization	pressurization	NOUN
cet-3413	90	10	due	due	ADP
cet-3413	90	11	to	to	ADP
cet-3413	90	12	the	the	DET
cet-3413	90	13	high	high	ADJ
cet-3413	90	14	vapour	vapour	NOUN
cet-3413	90	15	pressure	pressure	NOUN
cet-3413	90	16	caused	cause	VERB
cet-3413	90	17	by	by	ADP
cet-3413	90	18	exceeding	exceed	VERB
cet-3413	90	19	the	the	DET
cet-3413	90	20	boiling	boiling	NOUN
cet-3413	90	21	point	point	NOUN
cet-3413	90	22	of	of	ADP
cet-3413	90	23	dichloromethane	dichloromethane	NOUN
cet-3413	90	24	and	and	CCONJ
cet-3413	90	25	the	the	DET
cet-3413	90	26	formation	formation	NOUN
cet-3413	90	27	of	of	ADP
cet-3413	90	28	permanent	permanent	ADJ
cet-3413	90	29	gas	gas	NOUN
cet-3413	90	30	during	during	ADP
cet-3413	90	31	the	the	DET
cet-3413	90	32	decomposition	decomposition	NOUN
cet-3413	90	33	,	,	PUNCT
cet-3413	90	34	as	as	SCONJ
cet-3413	90	35	seen	see	VERB
cet-3413	90	36	in	in	ADP
cet-3413	90	37	the	the	DET
cet-3413	90	38	blown	blow	VERB
cet-3413	90	39	up	up	ADP
cet-3413	90	40	waste	waste	NOUN
cet-3413	90	41	drum	drum	NOUN
cet-3413	90	42	filled	fill	VERB
cet-3413	90	43	with	with	ADP
cet-3413	90	44	dichloromethane	dichloromethane	NOUN
cet-3413	90	45	and	and	CCONJ
cet-3413	90	46	morpholine	morpholine	NOUN
cet-3413	90	47	(	(	PUNCT
cet-3413	90	48	neuenfeld	neuenfeld	ADJ
cet-3413	90	49	,	,	PUNCT
cet-3413	90	50	2008	2008	NUM
cet-3413	90	51	)	)	PUNCT
cet-3413	90	52	.	.	PUNCT
cet-3413	91	1	reference	reference	NOUN
cet-3413	91	2	heskey	heskey	PROPN
cet-3413	91	3	,	,	PUNCT
cet-3413	91	4	w.a	w.a	PROPN
cet-3413	91	5	.	.	PROPN
cet-3413	91	6	,	,	PUNCT
cet-3413	91	7	1986	1986	NUM
cet-3413	91	8	,	,	PUNCT
cet-3413	91	9	chem	chem	NOUN
cet-3413	91	10	.	.	PUNCT
cet-3413	92	1	eng	eng	PROPN
cet-3413	92	2	.	.	PUNCT
cet-3413	93	1	news	news	PROPN
cet-3413	93	2	,	,	PUNCT
cet-3413	93	3	64(21	64(21	NOUN
cet-3413	93	4	)	)	PUNCT
cet-3413	93	5	,	,	PUNCT
cet-3413	93	6	2	2	NUM
cet-3413	93	7	,	,	PUNCT
cet-3413	93	8	doi	doi	NOUN
cet-3413	93	9	:	:	PUNCT
cet-3413	93	10	10.1021	10.1021	NUM
cet-3413	93	11	/	/	SYM
cet-3413	93	12	cen	cen	PROPN
cet-3413	93	13	-	-	PUNCT
cet-3413	93	14	v064n021	v064n021	NOUN
cet-3413	93	15	neuenfeld	neuenfeld	ADJ
cet-3413	93	16	s.	s.	PROPN
cet-3413	93	17	,	,	PUNCT
cet-3413	93	18	2008	2008	NUM
cet-3413	93	19	,	,	PUNCT
cet-3413	93	20	incident	incident	NOUN
cet-3413	93	21	report	report	NOUN
cet-3413	93	22	the	the	DET
cet-3413	93	23	flying	fly	VERB
cet-3413	93	24	waste	waste	NOUN
cet-3413	93	25	drum	drum	NOUN
cet-3413	93	26	an	an	DET
cet-3413	93	27	unexpected	unexpected	ADJ
cet-3413	93	28	reaction	reaction	NOUN
cet-3413	93	29	between	between	ADP
cet-3413	93	30	methylene	methylene	NOUN
cet-3413	93	31	chloride	chloride	NOUN
cet-3413	93	32	and	and	CCONJ
cet-3413	93	33	morpholine	morpholine	NOUN
cet-3413	93	34	.	.	PUNCT
cet-3413	94	1	iwg	iwg	PROPN
cet-3413	94	2	-	-	PUNCT
cet-3413	94	3	meeting	meeting	NOUN
cet-3413	94	4	at	at	ADP
cet-3413	94	5	basf	basf	PROPN
cet-3413	94	6	,	,	PUNCT
cet-3413	94	7	ludwigshafen	ludwigshafen	PROPN
cet-3413	94	8	,	,	PUNCT
cet-3413	94	9	germany	germany	PROPN
cet-3413	94	10	nolan	nolan	PROPN
cet-3413	94	11	,	,	PUNCT
cet-3413	94	12	1983	1983	NUM
cet-3413	94	13	,	,	PUNCT
cet-3413	94	14	case	case	NOUN
cet-3413	94	15	history	history	NOUN
cet-3413	94	16	145	145	NUM
cet-3413	94	17	urben	urben	NOUN
cet-3413	94	18	p.g	p.g	PROPN
cet-3413	94	19	.	.	PROPN
cet-3413	94	20	,	,	PUNCT
cet-3413	94	21	2007	2007	NUM
cet-3413	94	22	,	,	PUNCT
cet-3413	94	23	bretherick	bretherick	PROPN
cet-3413	94	24	’s	’s	PART
cet-3413	94	25	handbook	handbook	NOUN
cet-3413	94	26	of	of	ADP
cet-3413	94	27	reactive	reactive	ADJ
cet-3413	94	28	chemical	chemical	NOUN
cet-3413	94	29	hazards	hazard	NOUN
cet-3413	94	30	,	,	PUNCT
cet-3413	94	31	vol	vol	NOUN
cet-3413	94	32	.	.	PROPN
cet-3413	94	33	1	1	NUM
cet-3413	94	34	,	,	PUNCT
cet-3413	94	35	7th	7th	ADJ
cet-3413	94	36	edition	edition	NOUN
cet-3413	94	37	,	,	PUNCT
cet-3413	94	38	174	174	NUM
cet-3413	94	39	.	.	PUNCT
cet-3413	95	1	elsevier	elsevier	PROPN
cet-3413	95	2	,	,	PUNCT
cet-3413	95	3	amsterdam	amsterdam	PROPN
cet-3413	95	4	,	,	PUNCT
cet-3413	95	5	the	the	DET
cet-3413	95	6	netherlands	netherlands	PROPN
cet-3413	95	7	768	768	NUM