id	author	title	date	pages	extension	mime	words	sentence	flesch	summary	cache	txt
ecletica-233	Locatelli, José Roberto; de Carvalho, Cláudio Teodoro; Caires, Flávio Junior; Ionashiro, Massao	Synthesis, characterization and thermal behaviour of heavy trivalent lanthanide malonates	2010	8	.pdf	application/pdf	3826	162	65	These curves also show that the first mass loss occurs within the same temperature range for Tb, Dy, Ho and Tm compounds (i.e. 303 – 473 K) and for Er, Yb and Lu ones (i.e. 303 – 453 K), in spite of the compounds have been maintained in a forced circulation oven at 323 K during 12 h and removed to a desiccator over anhydrous calcium chloride. In this paper, the object of the present research was to prepare solid state compounds of heavy trivalent lanthanide ions (i.e. Tb to Lu) with malonate and to characterize and to investigate by means of complexometry, elemental analysis, X-ray powder diffractometry, infrared spectroscopy, simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC) and TG-FTIR system.	cache/ecletica-233.pdf	txt/ecletica-233.txt