id	sid	tid	token	lemma	pos
ecletica-204	1	1	eclética	eclética	PROPN
ecletica-204	1	2	química	química	PROPN
ecletica-204	1	3	35-3.indd	35-3.indd	NUM
ecletica-204	1	4	eclética	eclética	PROPN
ecletica-204	1	5	química	química	PROPN
ecletica-204	1	6	www.scielo.br/eq	www.scielo.br/eq	PROPN
ecletica-204	1	7	volume	volume	NOUN
ecletica-204	1	8	35	35	NUM
ecletica-204	1	9	,	,	PUNCT
ecletica-204	1	10	número	número	NOUN
ecletica-204	1	11	3	3	NUM
ecletica-204	1	12	,	,	PUNCT
ecletica-204	1	13	2010	2010	NUM
ecletica-204	1	14	45	45	NUM
ecletica-204	1	15	artigo	artigo	PROPN
ecletica-204	1	16	/	/	SYM
ecletica-204	1	17	article	article	NOUN
ecletica-204	1	18	development	development	NOUN
ecletica-204	1	19	and	and	CCONJ
ecletica-204	1	20	validation	validation	NOUN
ecletica-204	1	21	of	of	ADP
ecletica-204	1	22	spectrophotometric	spectrophotometric	ADJ
ecletica-204	1	23	method	method	NOUN
ecletica-204	1	24	for	for	ADP
ecletica-204	1	25	the	the	DET
ecletica-204	1	26	determination	determination	NOUN
ecletica-204	1	27	of	of	ADP
ecletica-204	1	28	dpp-4	dpp-4	ADJ
ecletica-204	1	29	inhibitor	inhibitor	NOUN
ecletica-204	1	30	,	,	PUNCT
ecletica-204	1	31	sitagliptin	sitagliptin	NOUN
ecletica-204	1	32	,	,	PUNCT
ecletica-204	1	33	in	in	ADP
ecletica-204	1	34	its	its	PRON
ecletica-204	1	35	pharmaceutical	pharmaceutical	ADJ
ecletica-204	1	36	preparations	preparation	NOUN
ecletica-204	1	37	c.	c.	PROPN
ecletica-204	1	38	bala	bala	PROPN
ecletica-204	1	39	sekaran1	sekaran1	PROPN
ecletica-204	1	40	*	*	PUNCT
ecletica-204	1	41	,	,	PUNCT
ecletica-204	1	42	a.	a.	NOUN
ecletica-204	1	43	prameela	prameela	PROPN
ecletica-204	1	44	rani2	rani2	NOUN
ecletica-204	1	45	1	1	NUM
ecletica-204	1	46	department	department	NOUN
ecletica-204	1	47	of	of	ADP
ecletica-204	1	48	biotechnology	biotechnology	NOUN
ecletica-204	1	49	,	,	PUNCT
ecletica-204	1	50	j.	j.	PROPN
ecletica-204	1	51	k.	k.	PROPN
ecletica-204	1	52	c.	c.	PROPN
ecletica-204	1	53	college	college	PROPN
ecletica-204	1	54	,	,	PUNCT
ecletica-204	1	55	guntur	guntur	PROPN
ecletica-204	1	56	,	,	PUNCT
ecletica-204	1	57	india	india	PROPN
ecletica-204	1	58	.	.	PROPN
ecletica-204	1	59	2	2	NUM
ecletica-204	1	60	department	department	NOUN
ecletica-204	1	61	of	of	ADP
ecletica-204	1	62	pharmaceutics	pharmaceutic	NOUN
ecletica-204	1	63	,	,	PUNCT
ecletica-204	1	64	k.v.s.r	k.v.s.r	PROPN
ecletica-204	1	65	.	.	PROPN
ecletica-204	1	66	siddhartha	siddhartha	PROPN
ecletica-204	1	67	college	college	PROPN
ecletica-204	1	68	of	of	ADP
ecletica-204	1	69	pharmaceutical	pharmaceutical	NOUN
ecletica-204	1	70	sciences	sciences	PROPN
ecletica-204	1	71	,	,	PUNCT
ecletica-204	1	72	vijayawada	vijayawada	PROPN
ecletica-204	1	73	,	,	PUNCT
ecletica-204	1	74	india	india	PROPN
ecletica-204	1	75	.	.	PUNCT
ecletica-204	2	1	*	*	PUNCT
ecletica-204	2	2	corresponding	correspond	VERB
ecletica-204	2	3	author	author	NOUN
ecletica-204	2	4	:	:	PUNCT
ecletica-204	2	5	c.	c.	PROPN
ecletica-204	2	6	bala	bala	PROPN
ecletica-204	2	7	sekaran	sekaran	PROPN
ecletica-204	2	8	,	,	PUNCT
ecletica-204	2	9	20	20	NUM
ecletica-204	2	10	-	-	SYM
ecletica-204	2	11	3/2	3/2	NUM
ecletica-204	2	12	-	-	PUNCT
ecletica-204	2	13	5	5	NUM
ecletica-204	2	14	,	,	PUNCT
ecletica-204	2	15	ii	ii	NOUN
ecletica-204	2	16	floor	floor	NOUN
ecletica-204	2	17	,	,	PUNCT
ecletica-204	2	18	ramalayam	ramalayam	PROPN
ecletica-204	2	19	street	street	PROPN
ecletica-204	2	20	,	,	PUNCT
ecletica-204	2	21	ayodhya	ayodhya	NOUN
ecletica-204	2	22	nagar	nagar	NOUN
ecletica-204	2	23	,	,	PUNCT
ecletica-204	2	24	vijayawada	vijayawada	PROPN
ecletica-204	2	25	–	–	PUNCT
ecletica-204	2	26	520	520	NUM
ecletica-204	2	27	003	003	NUM
ecletica-204	2	28	.	.	PROPN
ecletica-204	2	29	andhra	andhra	PROPN
ecletica-204	2	30	pradesh	pradesh	PROPN
ecletica-204	2	31	.	.	PUNCT
ecletica-204	3	1	e	e	X
ecletica-204	3	2	-	-	NOUN
ecletica-204	3	3	mail	mail	NOUN
ecletica-204	3	4	:	:	PUNCT
ecletica-204	3	5	balumphil@gmail.com	balumphil@gmail.com	X
ecletica-204	4	1	call	call	NOUN
ecletica-204	4	2	:	:	PUNCT
ecletica-204	4	3	91	91	NUM
ecletica-204	4	4	-	-	PUNCT
ecletica-204	4	5	866	866	NUM
ecletica-204	4	6	-	-	PUNCT
ecletica-204	4	7	2538492	2538492	NUM
ecletica-204	4	8	abstract	abstract	NOUN
ecletica-204	4	9	:	:	PUNCT
ecletica-204	4	10	a	a	DET
ecletica-204	4	11	simple	simple	ADJ
ecletica-204	4	12	,	,	PUNCT
ecletica-204	4	13	sensitive	sensitive	ADJ
ecletica-204	4	14	and	and	CCONJ
ecletica-204	4	15	reproducible	reproducible	ADJ
ecletica-204	4	16	spectrophotometric	spectrophotometric	ADJ
ecletica-204	4	17	method	method	NOUN
ecletica-204	4	18	was	be	AUX
ecletica-204	4	19	developed	develop	VERB
ecletica-204	4	20	for	for	ADP
ecletica-204	4	21	the	the	DET
ecletica-204	4	22	determination	determination	NOUN
ecletica-204	4	23	of	of	ADP
ecletica-204	4	24	sitagliptin	sitagliptin	NOUN
ecletica-204	4	25	phosphate	phosphate	NOUN
ecletica-204	4	26	in	in	ADP
ecletica-204	4	27	bulk	bulk	NOUN
ecletica-204	4	28	and	and	CCONJ
ecletica-204	4	29	in	in	ADP
ecletica-204	4	30	pharmaceutical	pharmaceutical	NOUN
ecletica-204	4	31	formulations	formulation	NOUN
ecletica-204	4	32	.	.	PUNCT
ecletica-204	5	1	the	the	DET
ecletica-204	5	2	proposed	propose	VERB
ecletica-204	5	3	method	method	NOUN
ecletica-204	5	4	is	be	AUX
ecletica-204	5	5	based	base	VERB
ecletica-204	5	6	on	on	ADP
ecletica-204	5	7	condensation	condensation	NOUN
ecletica-204	5	8	of	of	ADP
ecletica-204	5	9	the	the	DET
ecletica-204	5	10	primary	primary	ADJ
ecletica-204	5	11	amino	amino	NOUN
ecletica-204	5	12	group	group	NOUN
ecletica-204	5	13	of	of	ADP
ecletica-204	5	14	sitagliptin	sitagliptin	NOUN
ecletica-204	5	15	phosphate	phosphate	NOUN
ecletica-204	5	16	with	with	ADP
ecletica-204	5	17	acetyl	acetyl	NOUN
ecletica-204	5	18	acetone	acetone	NOUN
ecletica-204	5	19	and	and	CCONJ
ecletica-204	5	20	formaldehyde	formaldehyde	NOUN
ecletica-204	5	21	producing	produce	VERB
ecletica-204	5	22	a	a	DET
ecletica-204	5	23	yellow	yellow	ADJ
ecletica-204	5	24	colored	colored	ADJ
ecletica-204	5	25	product	product	NOUN
ecletica-204	5	26	,	,	PUNCT
ecletica-204	5	27	which	which	PRON
ecletica-204	5	28	is	be	AUX
ecletica-204	5	29	measured	measure	VERB
ecletica-204	5	30	spectrophotometrically	spectrophotometrically	ADV
ecletica-204	5	31	at	at	ADP
ecletica-204	5	32	430	430	NUM
ecletica-204	5	33	nm	nm	NOUN
ecletica-204	5	34	.	.	PUNCT
ecletica-204	6	1	the	the	DET
ecletica-204	6	2	color	color	NOUN
ecletica-204	6	3	was	be	AUX
ecletica-204	6	4	stable	stable	ADJ
ecletica-204	6	5	for	for	ADP
ecletica-204	6	6	about	about	ADV
ecletica-204	6	7	1	1	NUM
ecletica-204	6	8	hour	hour	NOUN
ecletica-204	6	9	.	.	PUNCT
ecletica-204	7	1	beer	beer	NOUN
ecletica-204	7	2	’s	’s	PART
ecletica-204	7	3	law	law	NOUN
ecletica-204	7	4	is	be	AUX
ecletica-204	7	5	obeyed	obey	VERB
ecletica-204	7	6	over	over	ADP
ecletica-204	7	7	a	a	DET
ecletica-204	7	8	concentration	concentration	NOUN
ecletica-204	7	9	range	range	NOUN
ecletica-204	7	10	of	of	ADP
ecletica-204	7	11	5	5	NUM
ecletica-204	7	12	-	-	SYM
ecletica-204	7	13	25	25	NUM
ecletica-204	7	14	μg	μg	PROPN
ecletica-204	7	15	/	/	SYM
ecletica-204	7	16	ml	ml	PROPN
ecletica-204	7	17	.	.	PUNCT
ecletica-204	8	1	the	the	DET
ecletica-204	8	2	apparent	apparent	ADJ
ecletica-204	8	3	molar	molar	ADJ
ecletica-204	8	4	absorptivity	absorptivity	NOUN
ecletica-204	8	5	and	and	CCONJ
ecletica-204	8	6	sandell	sandell	NOUN
ecletica-204	8	7	sensitivity	sensitivity	NOUN
ecletica-204	8	8	values	value	NOUN
ecletica-204	8	9	are	be	AUX
ecletica-204	8	10	1.067	1.067	NUM
ecletica-204	8	11	x	x	SYM
ecletica-204	8	12	104	104	NUM
ecletica-204	8	13	lmol-1cm-1	lmol-1cm-1	NUM
ecletica-204	8	14	and	and	CCONJ
ecletica-204	8	15	0.0471	0.0471	NUM
ecletica-204	8	16	μgcm-2	μgcm-2	NUM
ecletica-204	8	17	respectively	respectively	ADV
ecletica-204	8	18	.	.	PUNCT
ecletica-204	9	1	all	all	DET
ecletica-204	9	2	the	the	DET
ecletica-204	9	3	variables	variable	NOUN
ecletica-204	9	4	were	be	AUX
ecletica-204	9	5	studied	study	VERB
ecletica-204	9	6	to	to	PART
ecletica-204	9	7	optimize	optimize	VERB
ecletica-204	9	8	the	the	DET
ecletica-204	9	9	reaction	reaction	NOUN
ecletica-204	9	10	conditions	condition	NOUN
ecletica-204	9	11	.	.	PUNCT
ecletica-204	10	1	no	no	DET
ecletica-204	10	2	interference	interference	NOUN
ecletica-204	10	3	was	be	AUX
ecletica-204	10	4	observed	observe	VERB
ecletica-204	10	5	in	in	ADP
ecletica-204	10	6	the	the	DET
ecletica-204	10	7	presence	presence	NOUN
ecletica-204	10	8	of	of	ADP
ecletica-204	10	9	common	common	ADJ
ecletica-204	10	10	pharmaceutical	pharmaceutical	ADJ
ecletica-204	10	11	excipients	excipient	NOUN
ecletica-204	10	12	.	.	PUNCT
ecletica-204	11	1	the	the	DET
ecletica-204	11	2	validity	validity	NOUN
ecletica-204	11	3	of	of	ADP
ecletica-204	11	4	the	the	DET
ecletica-204	11	5	method	method	NOUN
ecletica-204	11	6	was	be	AUX
ecletica-204	11	7	tested	test	VERB
ecletica-204	11	8	by	by	ADP
ecletica-204	11	9	analyzing	analyze	VERB
ecletica-204	11	10	sitagliptin	sitagliptin	NOUN
ecletica-204	11	11	phosphate	phosphate	NOUN
ecletica-204	11	12	in	in	ADP
ecletica-204	11	13	its	its	PRON
ecletica-204	11	14	pharmaceutical	pharmaceutical	ADJ
ecletica-204	11	15	preparations	preparation	NOUN
ecletica-204	11	16	.	.	PUNCT
ecletica-204	12	1	good	good	ADJ
ecletica-204	12	2	recoveries	recovery	NOUN
ecletica-204	12	3	were	be	AUX
ecletica-204	12	4	obtained	obtain	VERB
ecletica-204	12	5	.	.	PUNCT
ecletica-204	13	1	the	the	DET
ecletica-204	13	2	developed	develop	VERB
ecletica-204	13	3	method	method	NOUN
ecletica-204	13	4	was	be	AUX
ecletica-204	13	5	successfully	successfully	ADV
ecletica-204	13	6	employed	employ	VERB
ecletica-204	13	7	for	for	ADP
ecletica-204	13	8	the	the	DET
ecletica-204	13	9	determination	determination	NOUN
ecletica-204	13	10	of	of	ADP
ecletica-204	13	11	sitagliptin	sitagliptin	NOUN
ecletica-204	13	12	phosphate	phosphate	NOUN
ecletica-204	13	13	in	in	ADP
ecletica-204	13	14	various	various	ADJ
ecletica-204	13	15	pharmaceutical	pharmaceutical	ADJ
ecletica-204	13	16	preparations	preparation	NOUN
ecletica-204	13	17	.	.	PUNCT
ecletica-204	14	1	keywords	keyword	NOUN
ecletica-204	14	2	:	:	PUNCT
ecletica-204	14	3	sitagliptin	sitagliptin	NOUN
ecletica-204	14	4	phosphate	phosphate	NOUN
ecletica-204	14	5	,	,	PUNCT
ecletica-204	14	6	acetyl	acetyl	NOUN
ecletica-204	14	7	acetone	acetone	NOUN
ecletica-204	14	8	,	,	PUNCT
ecletica-204	14	9	beer	beer	NOUN
ecletica-204	14	10	’s	’s	PART
ecletica-204	14	11	law	law	NOUN
ecletica-204	14	12	,	,	PUNCT
ecletica-204	14	13	sandell	sandell	PROPN
ecletica-204	14	14	’s	’s	PART
ecletica-204	14	15	sensitivity	sensitivity	NOUN
ecletica-204	14	16	.	.	PUNCT
ecletica-204	15	1	introduction	introduction	NOUN
ecletica-204	15	2	sitagliptin	sitagliptin	NOUN
ecletica-204	15	3	phosphate(stp)(1	phosphate(stp)(1	PROPN
ecletica-204	15	4	-	-	PUNCT
ecletica-204	15	5	4	4	NUM
ecletica-204	15	6	)	)	PUNCT
ecletica-204	15	7	is	be	AUX
ecletica-204	15	8	1,2,4	1,2,4	NUM
ecletica-204	15	9	-	-	PUNCT
ecletica-204	15	10	triazolo[4,3	triazolo[4,3	NOUN
ecletica-204	15	11	-	-	PUNCT
ecletica-204	15	12	a]pyrazine,7-[(3r)-3	a]pyrazine,7-[(3r)-3	NOUN
ecletica-204	15	13	-	-	PUNCT
ecletica-204	15	14	amino-1	amino-1	NOUN
ecletica-204	15	15	-	-	PUNCT
ecletica-204	15	16	oxo-4-(2,4,5	oxo-4-(2,4,5	NOUN
ecletica-204	15	17	-	-	PUNCT
ecletica-204	15	18	trifluorophenyl)butyl]-5,6,7,8	trifluorophenyl)butyl]-5,6,7,8	NOUN
ecletica-204	15	19	-	-	PUNCT
ecletica-204	15	20	tetrahydro-3-(trifl	tetrahydro-3-(trifl	NOUN
ecletica-204	15	21	uoromethyl)-	uoromethyl)-	ADJ
ecletica-204	15	22	,	,	PUNCT
ecletica-204	15	23	phosphate	phosphate	ADJ
ecletica-204	15	24	,	,	PUNCT
ecletica-204	15	25	whose	whose	DET
ecletica-204	15	26	structure	structure	NOUN
ecletica-204	15	27	is	be	AUX
ecletica-204	15	28	given	give	VERB
ecletica-204	15	29	in	in	ADP
ecletica-204	15	30	the	the	DET
ecletica-204	15	31	fig	fig	NOUN
ecletica-204	15	32	.	.	PUNCT
ecletica-204	16	1	1	1	X
ecletica-204	16	2	.	.	X
ecletica-204	17	1	it	it	PRON
ecletica-204	17	2	is	be	AUX
ecletica-204	17	3	used	use	VERB
ecletica-204	17	4	in	in	ADP
ecletica-204	17	5	the	the	DET
ecletica-204	17	6	treatment	treatment	NOUN
ecletica-204	17	7	of	of	ADP
ecletica-204	17	8	diabetes	diabetes	NOUN
ecletica-204	17	9	.	.	PUNCT
ecletica-204	18	1	it	it	PRON
ecletica-204	18	2	is	be	AUX
ecletica-204	18	3	an	an	DET
ecletica-204	18	4	oral	oral	ADJ
ecletica-204	18	5	antihyperglycemic	antihyperglycemic	ADJ
ecletica-204	18	6	(	(	PUNCT
ecletica-204	18	7	anti	anti	ADJ
ecletica-204	18	8	-	-	ADJ
ecletica-204	18	9	diabetic	diabetic	ADJ
ecletica-204	18	10	)	)	PUNCT
ecletica-204	18	11	drug	drug	NOUN
ecletica-204	18	12	of	of	ADP
ecletica-204	18	13	the	the	DET
ecletica-204	18	14	dipeptidyl	dipeptidyl	NOUN
ecletica-204	18	15	peptidase-4	peptidase-4	NOUN
ecletica-204	18	16	(	(	PUNCT
ecletica-204	18	17	dpp-4	dpp-4	NUM
ecletica-204	18	18	)	)	PUNCT
ecletica-204	18	19	inhibitor	inhibitor	NOUN
ecletica-204	18	20	class	class	NOUN
ecletica-204	18	21	.	.	PUNCT
ecletica-204	19	1	literature	literature	NOUN
ecletica-204	19	2	survey	survey	NOUN
ecletica-204	19	3	reveals	reveal	VERB
ecletica-204	19	4	that	that	SCONJ
ecletica-204	19	5	only	only	ADV
ecletica-204	19	6	lc	lc	PROPN
ecletica-204	19	7	-	-	PUNCT
ecletica-204	19	8	ms	ms	NOUN
ecletica-204	19	9	(	(	PUNCT
ecletica-204	19	10	5	5	NUM
ecletica-204	19	11	-	-	SYM
ecletica-204	19	12	8)	8)	NUM
ecletica-204	19	13	methods	method	NOUN
ecletica-204	19	14	were	be	AUX
ecletica-204	19	15	reported	report	VERB
ecletica-204	19	16	for	for	ADP
ecletica-204	19	17	the	the	DET
ecletica-204	19	18	determination	determination	NOUN
ecletica-204	19	19	of	of	ADP
ecletica-204	19	20	sitagliptin	sitagliptin	NOUN
ecletica-204	19	21	phosphate	phosphate	NOUN
ecletica-204	19	22	in	in	ADP
ecletica-204	19	23	plasma	plasma	NOUN
ecletica-204	19	24	and	and	CCONJ
ecletica-204	19	25	urine	urine	NOUN
ecletica-204	19	26	of	of	ADP
ecletica-204	19	27	humans	human	NOUN
ecletica-204	19	28	,	,	PUNCT
ecletica-204	19	29	rats	rat	NOUN
ecletica-204	19	30	and	and	CCONJ
ecletica-204	19	31	dogs	dog	NOUN
ecletica-204	19	32	.	.	PUNCT
ecletica-204	20	1	so	so	ADV
ecletica-204	20	2	far	far	ADV
ecletica-204	20	3	,	,	PUNCT
ecletica-204	20	4	no	no	DET
ecletica-204	20	5	assay	assay	NOUN
ecletica-204	20	6	procedure	procedure	NOUN
ecletica-204	20	7	has	have	AUX
ecletica-204	20	8	been	be	AUX
ecletica-204	20	9	reported	report	VERB
ecletica-204	20	10	for	for	ADP
ecletica-204	20	11	the	the	DET
ecletica-204	20	12	determination	determination	NOUN
ecletica-204	20	13	of	of	ADP
ecletica-204	20	14	this	this	DET
ecletica-204	20	15	drug	drug	NOUN
ecletica-204	20	16	in	in	ADP
ecletica-204	20	17	its	its	PRON
ecletica-204	20	18	pharmaceutical	pharmaceutical	NOUN
ecletica-204	20	19	formulations	formulation	NOUN
ecletica-204	20	20	.	.	PUNCT
ecletica-204	21	1	among	among	ADP
ecletica-204	21	2	the	the	DET
ecletica-204	21	3	various	various	ADJ
ecletica-204	21	4	methods	method	NOUN
ecletica-204	21	5	available	available	ADJ
ecletica-204	21	6	for	for	ADP
ecletica-204	21	7	the	the	DET
ecletica-204	21	8	determination	determination	NOUN
ecletica-204	21	9	of	of	ADP
ecletica-204	21	10	drugs	drug	NOUN
ecletica-204	21	11	,	,	PUNCT
ecletica-204	21	12	spectrophotometry	spectrophotometry	NOUN
ecletica-204	21	13	continues	continue	VERB
ecletica-204	21	14	to	to	PART
ecletica-204	21	15	be	be	AUX
ecletica-204	21	16	very	very	ADV
ecletica-204	21	17	popular	popular	ADJ
ecletica-204	21	18	,	,	PUNCT
ecletica-204	21	19	because	because	SCONJ
ecletica-204	21	20	of	of	ADP
ecletica-204	21	21	their	their	PRON
ecletica-204	21	22	simplicity	simplicity	NOUN
ecletica-204	21	23	,	,	PUNCT
ecletica-204	21	24	specifi	specifi	PROPN
ecletica-204	21	25	city	city	PROPN
ecletica-204	21	26	and	and	CCONJ
ecletica-204	21	27	low	low	ADJ
ecletica-204	21	28	cost	cost	NOUN
ecletica-204	21	29	.	.	PUNCT
ecletica-204	22	1	this	this	DET
ecletica-204	22	2	study	study	NOUN
ecletica-204	22	3	presents	present	VERB
ecletica-204	22	4	new	new	ADJ
ecletica-204	22	5	spectrophotometric	spectrophotometric	ADJ
ecletica-204	22	6	method	method	NOUN
ecletica-204	22	7	for	for	ADP
ecletica-204	22	8	the	the	DET
ecletica-204	22	9	determination	determination	NOUN
ecletica-204	22	10	of	of	ADP
ecletica-204	22	11	sitagliptin	sitagliptin	NOUN
ecletica-204	22	12	phosphate	phosphate	NOUN
ecletica-204	22	13	in	in	ADP
ecletica-204	22	14	bulk	bulk	ADJ
ecletica-204	22	15	and	and	CCONJ
ecletica-204	22	16	pharmaceutical	pharmaceutical	NOUN
ecletica-204	22	17	formulations	formulation	NOUN
ecletica-204	22	18	.	.	PUNCT
ecletica-204	23	1	the	the	DET
ecletica-204	23	2	developed	develop	VERB
ecletica-204	23	3	method	method	NOUN
ecletica-204	23	4	is	be	AUX
ecletica-204	23	5	based	base	VERB
ecletica-204	23	6	on	on	ADP
ecletica-204	23	7	the	the	DET
ecletica-204	23	8	reaction	reaction	NOUN
ecletica-204	23	9	of	of	ADP
ecletica-204	23	10	sitagliptin	sitagliptin	NOUN
ecletica-204	23	11	phosphate	phosphate	NOUN
ecletica-204	23	12	with	with	ADP
ecletica-204	23	13	acetyl	acetyl	NOUN
ecletica-204	23	14	acetone	acetone	NOUN
ecletica-204	23	15	and	and	CCONJ
ecletica-204	23	16	formaldehyde	formaldehyde	NOUN
ecletica-204	23	17	producing	produce	VERB
ecletica-204	23	18	hantzsch	hantzsch	ADJ
ecletica-204	23	19	product	product	NOUN
ecletica-204	23	20	.	.	PUNCT
ecletica-204	24	1	ecl	ecl	PROPN
ecletica-204	24	2	.	.	PROPN
ecletica-204	24	3	quím	quím	PROPN
ecletica-204	24	4	.	.	PUNCT
ecletica-204	24	5	,	,	PUNCT
ecletica-204	24	6	são	são	PROPN
ecletica-204	24	7	paulo	paulo	PROPN
ecletica-204	24	8	,	,	PUNCT
ecletica-204	24	9	35	35	NUM
ecletica-204	24	10	3	3	NUM
ecletica-204	24	11	:	:	PUNCT
ecletica-204	24	12	45	45	NUM
ecletica-204	24	13	53	53	NUM
ecletica-204	24	14	,	,	PUNCT
ecletica-204	25	1	2010	2010	NUM
ecletica-204	25	2	ecl	ecl	PROPN
ecletica-204	25	3	.	.	PROPN
ecletica-204	25	4	quím	quím	PROPN
ecletica-204	25	5	.	.	PUNCT
ecletica-204	25	6	,	,	PUNCT
ecletica-204	25	7	são	são	PROPN
ecletica-204	25	8	paulo	paulo	PROPN
ecletica-204	25	9	,	,	PUNCT
ecletica-204	25	10	35	35	NUM
ecletica-204	25	11	3	3	NUM
ecletica-204	25	12	:	:	PUNCT
ecletica-204	25	13	45	45	NUM
ecletica-204	25	14	53	53	NUM
ecletica-204	25	15	,	,	PUNCT
ecletica-204	25	16	201046	201046	NUM
ecletica-204	25	17	ecl	ecl	PROPN
ecletica-204	25	18	.	.	PROPN
ecletica-204	25	19	quím	quím	PROPN
ecletica-204	25	20	.	.	PUNCT
ecletica-204	25	21	,	,	PUNCT
ecletica-204	25	22	são	são	PROPN
ecletica-204	25	23	paulo	paulo	PROPN
ecletica-204	25	24	,	,	PUNCT
ecletica-204	25	25	35	35	NUM
ecletica-204	25	26	3	3	NUM
ecletica-204	25	27	:	:	PUNCT
ecletica-204	25	28	45	45	NUM
ecletica-204	25	29	53	53	NUM
ecletica-204	25	30	,	,	PUNCT
ecletica-204	25	31	2010	2010	NUM
ecletica-204	25	32	47	47	NUM
ecletica-204	25	33	artigo	artigo	NOUN
ecletica-204	25	34	article	article	NOUN
ecletica-204	25	35	artigo	artigo	PROPN
ecletica-204	25	36	article	article	PROPN
ecletica-204	25	37	fig	fig	NOUN
ecletica-204	25	38	1	1	NUM
ecletica-204	25	39	.	.	PUNCT
ecletica-204	26	1	sitagliptin	sitagliptin	NOUN
ecletica-204	26	2	phosphate	phosphate	ADJ
ecletica-204	26	3	experimental	experimental	ADJ
ecletica-204	26	4	apparatus	apparatus	NOUN
ecletica-204	26	5	•	•	ADP
ecletica-204	26	6	spectral	spectral	ADJ
ecletica-204	26	7	and	and	CCONJ
ecletica-204	26	8	absorbance	absorbance	NOUN
ecletica-204	26	9	measurements	measurement	NOUN
ecletica-204	26	10	were	be	AUX
ecletica-204	26	11	carried	carry	VERB
ecletica-204	26	12	out	out	ADP
ecletica-204	26	13	by	by	ADP
ecletica-204	26	14	using	use	VERB
ecletica-204	26	15	systronics	systronic	NOUN
ecletica-204	26	16	uv	uv	NOUN
ecletica-204	26	17	–	–	PUNCT
ecletica-204	26	18	visible	visible	ADJ
ecletica-204	26	19	double	double	ADJ
ecletica-204	26	20	beam	beam	NOUN
ecletica-204	26	21	spectrophotometer	spectrophotometer	NOUN
ecletica-204	26	22	model	model	NOUN
ecletica-204	26	23	2201	2201	NUM
ecletica-204	26	24	.	.	PUNCT
ecletica-204	27	1	•	•	NUM
ecletica-204	27	2	systronics	systronic	NOUN
ecletica-204	27	3	digital	digital	ADJ
ecletica-204	27	4	ph	ph	ADJ
ecletica-204	27	5	meter	meter	NOUN
ecletica-204	27	6	was	be	AUX
ecletica-204	27	7	used	use	VERB
ecletica-204	27	8	to	to	PART
ecletica-204	27	9	adjust	adjust	VERB
ecletica-204	27	10	and	and	CCONJ
ecletica-204	27	11	determine	determine	VERB
ecletica-204	27	12	the	the	DET
ecletica-204	27	13	hydrogen	hydrogen	NOUN
ecletica-204	27	14	ion	ion	NOUN
ecletica-204	27	15	concentration	concentration	NOUN
ecletica-204	27	16	(	(	PUNCT
ecletica-204	27	17	ph	ph	NOUN
ecletica-204	27	18	)	)	PUNCT
ecletica-204	27	19	of	of	ADP
ecletica-204	27	20	the	the	DET
ecletica-204	27	21	buffer	buffer	NOUN
ecletica-204	27	22	solution	solution	NOUN
ecletica-204	27	23	.	.	PUNCT
ecletica-204	28	1	materials	material	NOUN
ecletica-204	28	2	and	and	CCONJ
ecletica-204	28	3	reagents	reagent	NOUN
ecletica-204	28	4	:	:	PUNCT
ecletica-204	28	5	all	all	DET
ecletica-204	28	6	the	the	DET
ecletica-204	28	7	chemicals	chemical	NOUN
ecletica-204	28	8	used	use	VERB
ecletica-204	28	9	were	be	AUX
ecletica-204	28	10	of	of	ADP
ecletica-204	28	11	analytical	analytical	ADJ
ecletica-204	28	12	grade	grade	NOUN
ecletica-204	28	13	.	.	PUNCT
ecletica-204	29	1	all	all	DET
ecletica-204	29	2	the	the	DET
ecletica-204	29	3	solutions	solution	NOUN
ecletica-204	29	4	were	be	AUX
ecletica-204	29	5	freshly	freshly	ADV
ecletica-204	29	6	prepared	prepare	VERB
ecletica-204	29	7	in	in	ADP
ecletica-204	29	8	distilled	distil	VERB
ecletica-204	29	9	water	water	NOUN
ecletica-204	29	10	.	.	PUNCT
ecletica-204	30	1	•	•	NUM
ecletica-204	30	2	acetylacetone	acetylacetone	NOUN
ecletica-204	30	3	:	:	PUNCT
ecletica-204	30	4	8.4	8.4	NUM
ecletica-204	30	5	%	%	NOUN
ecletica-204	30	6	v	v	ADP
ecletica-204	30	7	/	/	SYM
ecletica-204	30	8	v	v	NOUN
ecletica-204	30	9	solution	solution	NOUN
ecletica-204	30	10	was	be	AUX
ecletica-204	30	11	freshly	freshly	ADV
ecletica-204	30	12	prepared	prepare	VERB
ecletica-204	30	13	by	by	ADP
ecletica-204	30	14	mixing	mix	VERB
ecletica-204	30	15	2.1	2.1	NUM
ecletica-204	30	16	ml	ml	NOUN
ecletica-204	30	17	of	of	ADP
ecletica-204	30	18	acetyl	acetyl	NOUN
ecletica-204	30	19	acetone	acetone	NOUN
ecletica-204	30	20	with	with	ADP
ecletica-204	30	21	10	10	NUM
ecletica-204	30	22	ml	ml	NOUN
ecletica-204	30	23	of	of	ADP
ecletica-204	30	24	acetate	acetate	NOUN
ecletica-204	30	25	buffer	buffer	NOUN
ecletica-204	30	26	(	(	PUNCT
ecletica-204	30	27	ph	ph	NOUN
ecletica-204	30	28	5	5	NUM
ecletica-204	30	29	)	)	PUNCT
ecletica-204	30	30	and	and	CCONJ
ecletica-204	30	31	diluted	dilute	VERB
ecletica-204	30	32	to	to	ADP
ecletica-204	30	33	25	25	NUM
ecletica-204	30	34	ml	ml	NOUN
ecletica-204	30	35	with	with	ADP
ecletica-204	30	36	distilled	distil	VERB
ecletica-204	30	37	water	water	NOUN
ecletica-204	30	38	.	.	PUNCT
ecletica-204	31	1	•	•	NUM
ecletica-204	31	2	formaldehyde	formaldehyde	NOUN
ecletica-204	31	3	(	(	PUNCT
ecletica-204	31	4	34	34	NUM
ecletica-204	31	5	40	40	NUM
ecletica-204	31	6	%	%	NOUN
ecletica-204	31	7	):	):	PUNCT
ecletica-204	31	8	twenty	twenty	NUM
ecletica-204	31	9	percent	percent	NOUN
ecletica-204	31	10	solution	solution	NOUN
ecletica-204	31	11	was	be	AUX
ecletica-204	31	12	prepared	prepare	VERB
ecletica-204	31	13	by	by	ADP
ecletica-204	31	14	mixing	mix	VERB
ecletica-204	31	15	5	5	NUM
ecletica-204	31	16	ml	ml	NOUN
ecletica-204	31	17	of	of	ADP
ecletica-204	31	18	formaldehyde	formaldehyde	NOUN
ecletica-204	31	19	with	with	ADP
ecletica-204	31	20	10ml	10ml	NOUN
ecletica-204	31	21	of	of	ADP
ecletica-204	31	22	acetate	acetate	NOUN
ecletica-204	31	23	buffer	buffer	NOUN
ecletica-204	31	24	(	(	PUNCT
ecletica-204	31	25	ph	ph	NOUN
ecletica-204	31	26	5	5	NUM
ecletica-204	31	27	)	)	PUNCT
ecletica-204	31	28	and	and	CCONJ
ecletica-204	31	29	diluted	dilute	VERB
ecletica-204	31	30	to	to	ADP
ecletica-204	31	31	25	25	NUM
ecletica-204	31	32	ml	ml	NOUN
ecletica-204	31	33	with	with	ADP
ecletica-204	31	34	distilled	distil	VERB
ecletica-204	31	35	water	water	NOUN
ecletica-204	31	36	.	.	PUNCT
ecletica-204	32	1	•	•	NOUN
ecletica-204	32	2	acetate	acetate	NOUN
ecletica-204	32	3	buffer	buffer	NOUN
ecletica-204	32	4	(	(	PUNCT
ecletica-204	32	5	ph	ph	NOUN
ecletica-204	32	6	5	5	NUM
ecletica-204	32	7	):	):	PUNCT
ecletica-204	32	8	prepared	prepare	VERB
ecletica-204	32	9	by	by	ADP
ecletica-204	32	10	dissolving	dissolve	VERB
ecletica-204	32	11	13.6	13.6	NUM
ecletica-204	32	12	g	g	NOUN
ecletica-204	32	13	of	of	ADP
ecletica-204	32	14	sodium	sodium	NOUN
ecletica-204	32	15	acetate	acetate	NOUN
ecletica-204	32	16	and	and	CCONJ
ecletica-204	32	17	6	6	NUM
ecletica-204	32	18	ml	ml	NOUN
ecletica-204	32	19	of	of	ADP
ecletica-204	32	20	glacial	glacial	ADJ
ecletica-204	32	21	acetic	acetic	ADJ
ecletica-204	32	22	acid	acid	NOUN
ecletica-204	32	23	in	in	ADP
ecletica-204	32	24	suffi	suffi	NOUN
ecletica-204	32	25	cient	cient	NOUN
ecletica-204	32	26	water	water	NOUN
ecletica-204	32	27	to	to	PART
ecletica-204	32	28	produce	produce	VERB
ecletica-204	32	29	1000	1000	NUM
ecletica-204	32	30	ml	ml	NOUN
ecletica-204	32	31	.	.	NOUN
ecletica-204	32	32	•	•	ADJ
ecletica-204	32	33	pharmaceutical	pharmaceutical	NOUN
ecletica-204	32	34	grade	grade	NOUN
ecletica-204	32	35	sitagliptin	sitagliptin	NOUN
ecletica-204	32	36	phosphate	phosphate	NOUN
ecletica-204	32	37	,	,	PUNCT
ecletica-204	32	38	certifi	certifi	PROPN
ecletica-204	32	39	ed	ed	NOUN
ecletica-204	32	40	to	to	PART
ecletica-204	32	41	be	be	AUX
ecletica-204	32	42	99.8	99.8	NUM
ecletica-204	32	43	%	%	NOUN
ecletica-204	32	44	pure	pure	ADJ
ecletica-204	32	45	was	be	AUX
ecletica-204	32	46	procured	procure	VERB
ecletica-204	32	47	from	from	ADP
ecletica-204	32	48	local	local	ADJ
ecletica-204	32	49	pharmaceutical	pharmaceutical	NOUN
ecletica-204	32	50	industry	industry	NOUN
ecletica-204	32	51	and	and	CCONJ
ecletica-204	32	52	was	be	AUX
ecletica-204	32	53	used	use	VERB
ecletica-204	32	54	as	as	SCONJ
ecletica-204	32	55	received	receive	VERB
ecletica-204	32	56	.	.	PUNCT
ecletica-204	33	1	•	•	NUM
ecletica-204	33	2	januvia	januvia	PROPN
ecletica-204	33	3	100	100	NUM
ecletica-204	33	4	mg	mg	PROPN
ecletica-204	33	5	,	,	PUNCT
ecletica-204	33	6	50	50	NUM
ecletica-204	33	7	mg	mg	NOUN
ecletica-204	33	8	and	and	CCONJ
ecletica-204	33	9	25	25	NUM
ecletica-204	33	10	mg	mg	PROPN
ecletica-204	33	11	(	(	PUNCT
ecletica-204	33	12	labeled	label	VERB
ecletica-204	33	13	to	to	PART
ecletica-204	33	14	contain	contain	VERB
ecletica-204	33	15	100	100	NUM
ecletica-204	33	16	mg	mg	NOUN
ecletica-204	33	17	,	,	PUNCT
ecletica-204	33	18	50	50	NUM
ecletica-204	33	19	mg	mg	NOUN
ecletica-204	33	20	and	and	CCONJ
ecletica-204	33	21	25	25	NUM
ecletica-204	33	22	mg	mg	NOUN
ecletica-204	33	23	of	of	ADP
ecletica-204	33	24	sitagliptin	sitagliptin	NOUN
ecletica-204	33	25	phosphate	phosphate	NOUN
ecletica-204	33	26	per	per	ADP
ecletica-204	33	27	tablet	tablet	NOUN
ecletica-204	33	28	)	)	PUNCT
ecletica-204	33	29	were	be	AUX
ecletica-204	33	30	obtained	obtain	VERB
ecletica-204	33	31	from	from	ADP
ecletica-204	33	32	the	the	DET
ecletica-204	33	33	local	local	ADJ
ecletica-204	33	34	pharmacy	pharmacy	NOUN
ecletica-204	33	35	.	.	PUNCT
ecletica-204	34	1	standard	standard	ADJ
ecletica-204	34	2	drug	drug	NOUN
ecletica-204	34	3	solution	solution	NOUN
ecletica-204	34	4	stock	stock	NOUN
ecletica-204	34	5	solution	solution	NOUN
ecletica-204	34	6	of	of	ADP
ecletica-204	34	7	stp	stp	X
ecletica-204	34	8	(	(	PUNCT
ecletica-204	34	9	1	1	NUM
ecletica-204	34	10	mg	mg	NUM
ecletica-204	34	11	/	/	SYM
ecletica-204	34	12	ml	ml	NOUN
ecletica-204	34	13	)	)	PUNCT
ecletica-204	34	14	was	be	AUX
ecletica-204	34	15	prepared	prepare	VERB
ecletica-204	34	16	by	by	ADP
ecletica-204	34	17	dissolving	dissolve	VERB
ecletica-204	34	18	100	100	NUM
ecletica-204	34	19	mg	mg	NOUN
ecletica-204	34	20	of	of	ADP
ecletica-204	34	21	stp	stp	PROPN
ecletica-204	34	22	in	in	ADP
ecletica-204	34	23	distilled	distil	VERB
ecletica-204	34	24	water	water	NOUN
ecletica-204	34	25	and	and	CCONJ
ecletica-204	34	26	making	make	VERB
ecletica-204	34	27	the	the	DET
ecletica-204	34	28	volume	volume	NOUN
ecletica-204	34	29	to	to	ADP
ecletica-204	34	30	100	100	NUM
ecletica-204	34	31	ml	ml	NOUN
ecletica-204	34	32	in	in	ADP
ecletica-204	34	33	a	a	DET
ecletica-204	34	34	standard	standard	ADJ
ecletica-204	34	35	volumetric	volumetric	NOUN
ecletica-204	34	36	fl	fl	NOUN
ecletica-204	34	37	ask	ask	VERB
ecletica-204	34	38	.	.	PUNCT
ecletica-204	35	1	working	work	VERB
ecletica-204	35	2	solution	solution	NOUN
ecletica-204	35	3	of	of	ADP
ecletica-204	35	4	lower	low	ADJ
ecletica-204	35	5	concentration	concentration	NOUN
ecletica-204	35	6	(	(	PUNCT
ecletica-204	35	7	100	100	NUM
ecletica-204	35	8	μg	μg	NOUN
ecletica-204	35	9	/	/	SYM
ecletica-204	35	10	ml	ml	NOUN
ecletica-204	35	11	)	)	PUNCT
ecletica-204	35	12	was	be	AUX
ecletica-204	35	13	prepared	prepare	VERB
ecletica-204	35	14	by	by	ADP
ecletica-204	35	15	further	further	ADJ
ecletica-204	35	16	dilution	dilution	NOUN
ecletica-204	35	17	of	of	ADP
ecletica-204	35	18	the	the	DET
ecletica-204	35	19	above	above	ADJ
ecletica-204	35	20	standard	standard	ADJ
ecletica-204	35	21	stock	stock	NOUN
ecletica-204	35	22	solution	solution	NOUN
ecletica-204	35	23	with	with	ADP
ecletica-204	35	24	water	water	NOUN
ecletica-204	35	25	.	.	PUNCT
ecletica-204	36	1	general	general	ADJ
ecletica-204	36	2	procedure	procedure	NOUN
ecletica-204	36	3	for	for	ADP
ecletica-204	36	4	the	the	DET
ecletica-204	36	5	determination	determination	NOUN
ecletica-204	36	6	of	of	ADP
ecletica-204	36	7	sitagliptin	sitagliptin	NOUN
ecletica-204	36	8	phosphate	phosphate	VERB
ecletica-204	36	9	different	different	ADJ
ecletica-204	36	10	aliquots	aliquot	NOUN
ecletica-204	36	11	of	of	ADP
ecletica-204	36	12	working	work	VERB
ecletica-204	36	13	standard	standard	ADJ
ecletica-204	36	14	solutions	solution	NOUN
ecletica-204	36	15	containing	contain	VERB
ecletica-204	36	16	50	50	NUM
ecletica-204	36	17	-	-	PUNCT
ecletica-204	36	18	250μg	250μg	NOUN
ecletica-204	36	19	of	of	ADP
ecletica-204	36	20	stp	stp	PROPN
ecletica-204	36	21	was	be	AUX
ecletica-204	36	22	transferred	transfer	VERB
ecletica-204	36	23	into	into	ADP
ecletica-204	36	24	a	a	DET
ecletica-204	36	25	series	series	NOUN
ecletica-204	36	26	of	of	ADP
ecletica-204	36	27	serially	serially	ADV
ecletica-204	36	28	numbered	number	VERB
ecletica-204	36	29	10ml	10ml	ADJ
ecletica-204	36	30	volumetric	volumetric	NOUN
ecletica-204	36	31	fl	fl	NOUN
ecletica-204	36	32	asks	ask	VERB
ecletica-204	36	33	.	.	PUNCT
ecletica-204	37	1	to	to	ADP
ecletica-204	37	2	each	each	DET
ecletica-204	37	3	fl	fl	NOUN
ecletica-204	37	4	ask	ask	VERB
ecletica-204	37	5	1	1	NUM
ecletica-204	37	6	ml	ml	NOUN
ecletica-204	37	7	of	of	ADP
ecletica-204	37	8	8.4	8.4	NUM
ecletica-204	37	9	%	%	NOUN
ecletica-204	37	10	v	v	ADP
ecletica-204	37	11	/	/	SYM
ecletica-204	37	12	v	v	NOUN
ecletica-204	37	13	acetyl	acetyl	NOUN
ecletica-204	37	14	acetone	acetone	NOUN
ecletica-204	37	15	solution	solution	NOUN
ecletica-204	37	16	and	and	CCONJ
ecletica-204	37	17	0.5	0.5	NUM
ecletica-204	37	18	ml	ml	NOUN
ecletica-204	37	19	of	of	ADP
ecletica-204	37	20	20	20	NUM
ecletica-204	37	21	%	%	NOUN
ecletica-204	37	22	formaldehyde	formaldehyde	NOUN
ecletica-204	37	23	reagents	reagent	NOUN
ecletica-204	37	24	were	be	AUX
ecletica-204	37	25	added	add	VERB
ecletica-204	37	26	.	.	PUNCT
ecletica-204	38	1	the	the	DET
ecletica-204	38	2	fl	fl	PROPN
ecletica-204	38	3	asks	ask	VERB
ecletica-204	38	4	were	be	AUX
ecletica-204	38	5	stoppered	stopper	VERB
ecletica-204	38	6	,	,	PUNCT
ecletica-204	38	7	contents	content	NOUN
ecletica-204	38	8	were	be	AUX
ecletica-204	38	9	mixed	mix	VERB
ecletica-204	38	10	well	well	ADV
ecletica-204	38	11	.	.	PUNCT
ecletica-204	39	1	the	the	DET
ecletica-204	39	2	mixture	mixture	NOUN
ecletica-204	39	3	was	be	AUX
ecletica-204	39	4	heated	heat	VERB
ecletica-204	39	5	for	for	ADP
ecletica-204	39	6	5	5	NUM
ecletica-204	39	7	min	min	NOUN
ecletica-204	39	8	,	,	PUNCT
ecletica-204	39	9	cooled	cool	VERB
ecletica-204	39	10	and	and	CCONJ
ecletica-204	39	11	diluted	dilute	VERB
ecletica-204	39	12	to	to	ADP
ecletica-204	39	13	10	10	NUM
ecletica-204	39	14	ml	ml	NOUN
ecletica-204	39	15	with	with	ADP
ecletica-204	39	16	distilled	distil	VERB
ecletica-204	39	17	water	water	NOUN
ecletica-204	39	18	.	.	PUNCT
ecletica-204	40	1	the	the	DET
ecletica-204	40	2	absorbance	absorbance	NOUN
ecletica-204	40	3	of	of	ADP
ecletica-204	40	4	the	the	DET
ecletica-204	40	5	yellow	yellow	ADJ
ecletica-204	40	6	color	color	NOUN
ecletica-204	40	7	solution	solution	NOUN
ecletica-204	40	8	was	be	AUX
ecletica-204	40	9	measured	measure	VERB
ecletica-204	40	10	at	at	ADP
ecletica-204	40	11	430	430	NUM
ecletica-204	40	12	nm	nm	NOUN
ecletica-204	40	13	using	use	VERB
ecletica-204	40	14	the	the	DET
ecletica-204	40	15	experiment	experiment	NOUN
ecletica-204	40	16	as	as	ADP
ecletica-204	40	17	a	a	DET
ecletica-204	40	18	blank	blank	NOUN
ecletica-204	40	19	.	.	PUNCT
ecletica-204	41	1	the	the	DET
ecletica-204	41	2	amount	amount	NOUN
ecletica-204	41	3	of	of	ADP
ecletica-204	41	4	sitagliptin	sitagliptin	NOUN
ecletica-204	41	5	phosphate	phosphate	NOUN
ecletica-204	41	6	present	present	NOUN
ecletica-204	41	7	in	in	ADP
ecletica-204	41	8	the	the	DET
ecletica-204	41	9	sample	sample	NOUN
ecletica-204	41	10	was	be	AUX
ecletica-204	41	11	computed	compute	VERB
ecletica-204	41	12	from	from	ADP
ecletica-204	41	13	the	the	DET
ecletica-204	41	14	corresponding	correspond	VERB
ecletica-204	41	15	calibration	calibration	NOUN
ecletica-204	41	16	curve	curve	NOUN
ecletica-204	41	17	.	.	PUNCT
ecletica-204	42	1	the	the	DET
ecletica-204	42	2	calibration	calibration	NOUN
ecletica-204	42	3	graph	graph	NOUN
ecletica-204	42	4	was	be	AUX
ecletica-204	42	5	prepared	prepare	VERB
ecletica-204	42	6	was	be	AUX
ecletica-204	42	7	prepared	prepare	VERB
ecletica-204	42	8	by	by	ADP
ecletica-204	42	9	plotting	plot	VERB
ecletica-204	42	10	absorbance	absorbance	NOUN
ecletica-204	42	11	versus	versus	ADP
ecletica-204	42	12	concentration	concentration	NOUN
ecletica-204	42	13	of	of	ADP
ecletica-204	42	14	drug	drug	NOUN
ecletica-204	42	15	and	and	CCONJ
ecletica-204	42	16	the	the	DET
ecletica-204	42	17	concentration	concentration	NOUN
ecletica-204	42	18	of	of	ADP
ecletica-204	42	19	the	the	DET
ecletica-204	42	20	unknown	unknown	NOUN
ecletica-204	42	21	was	be	AUX
ecletica-204	42	22	read	read	VERB
ecletica-204	42	23	from	from	ADP
ecletica-204	42	24	the	the	DET
ecletica-204	42	25	calibration	calibration	NOUN
ecletica-204	42	26	graph	graph	NOUN
ecletica-204	42	27	or	or	CCONJ
ecletica-204	42	28	computed	compute	VERB
ecletica-204	42	29	from	from	ADP
ecletica-204	42	30	the	the	DET
ecletica-204	42	31	regression	regression	NOUN
ecletica-204	42	32	equation	equation	NOUN
ecletica-204	42	33	derived	derive	VERB
ecletica-204	42	34	from	from	ADP
ecletica-204	42	35	the	the	DET
ecletica-204	42	36	beer	beer	NOUN
ecletica-204	42	37	’s	’s	PART
ecletica-204	42	38	law	law	NOUN
ecletica-204	42	39	data	datum	NOUN
ecletica-204	42	40	.	.	PUNCT
ecletica-204	43	1	the	the	DET
ecletica-204	43	2	calibration	calibration	NOUN
ecletica-204	43	3	graph	graph	NOUN
ecletica-204	43	4	was	be	AUX
ecletica-204	43	5	then	then	ADV
ecletica-204	43	6	prepared	prepare	VERB
ecletica-204	43	7	by	by	ADP
ecletica-204	43	8	plotting	plot	VERB
ecletica-204	43	9	the	the	DET
ecletica-204	43	10	absorbance	absorbance	NOUN
ecletica-204	43	11	versus	versus	ADP
ecletica-204	43	12	concentration	concentration	NOUN
ecletica-204	43	13	of	of	ADP
ecletica-204	43	14	the	the	DET
ecletica-204	43	15	drug	drug	NOUN
ecletica-204	43	16	assay	assay	NOUN
ecletica-204	43	17	procedure	procedure	NOUN
ecletica-204	43	18	for	for	ADP
ecletica-204	43	19	pharmaceutical	pharmaceutical	ADJ
ecletica-204	43	20	tablets	tablet	NOUN
ecletica-204	43	21	for	for	ADP
ecletica-204	43	22	the	the	DET
ecletica-204	43	23	analysis	analysis	NOUN
ecletica-204	43	24	of	of	ADP
ecletica-204	43	25	stp	stp	ADJ
ecletica-204	43	26	,	,	PUNCT
ecletica-204	43	27	three	three	NUM
ecletica-204	43	28	brands	brand	NOUN
ecletica-204	43	29	of	of	ADP
ecletica-204	43	30	commercially	commercially	ADV
ecletica-204	43	31	available	available	ADJ
ecletica-204	43	32	tablets	tablet	NOUN
ecletica-204	43	33	(	(	PUNCT
ecletica-204	43	34	20	20	NUM
ecletica-204	43	35	)	)	PUNCT
ecletica-204	43	36	were	be	AUX
ecletica-204	43	37	weighed	weigh	VERB
ecletica-204	43	38	and	and	CCONJ
ecletica-204	43	39	ground	grind	VERB
ecletica-204	43	40	into	into	ADP
ecletica-204	43	41	a	a	DET
ecletica-204	43	42	fi	fi	NOUN
ecletica-204	43	43	ne	ne	NOUN
ecletica-204	43	44	powder	powder	NOUN
ecletica-204	43	45	.	.	PUNCT
ecletica-204	44	1	an	an	DET
ecletica-204	44	2	accurately	accurately	ADV
ecletica-204	44	3	weighed	weigh	VERB
ecletica-204	44	4	portion	portion	NOUN
ecletica-204	44	5	of	of	ADP
ecletica-204	44	6	the	the	DET
ecletica-204	44	7	powder	powder	NOUN
ecletica-204	44	8	equivalent	equivalent	ADJ
ecletica-204	44	9	to	to	ADP
ecletica-204	44	10	100	100	NUM
ecletica-204	44	11	mg	mg	NUM
ecletica-204	44	12	of	of	ADP
ecletica-204	44	13	sitagliptin	sitagliptin	NOUN
ecletica-204	44	14	phosphate	phosphate	NOUN
ecletica-204	44	15	was	be	AUX
ecletica-204	44	16	transferred	transfer	VERB
ecletica-204	44	17	in	in	ADP
ecletica-204	44	18	to	to	ADP
ecletica-204	44	19	a	a	DET
ecletica-204	44	20	100ml	100ml	NOUN
ecletica-204	44	21	beaker	beaker	NOUN
ecletica-204	44	22	containing	contain	VERB
ecletica-204	44	23	small	small	ADJ
ecletica-204	44	24	volume	volume	NOUN
ecletica-204	44	25	of	of	ADP
ecletica-204	44	26	water	water	NOUN
ecletica-204	44	27	and	and	CCONJ
ecletica-204	44	28	the	the	DET
ecletica-204	44	29	solution	solution	NOUN
ecletica-204	44	30	was	be	AUX
ecletica-204	44	31	shaken	shake	VERB
ecletica-204	44	32	thoroughly	thoroughly	ADV
ecletica-204	44	33	for	for	ADP
ecletica-204	44	34	10	10	NUM
ecletica-204	44	35	-	-	SYM
ecletica-204	44	36	15	15	NUM
ecletica-204	44	37	minutes	minute	NOUN
ecletica-204	44	38	and	and	CCONJ
ecletica-204	44	39	fi	fi	NOUN
ecletica-204	44	40	ltered	ltere	VERB
ecletica-204	44	41	through	through	ADP
ecletica-204	44	42	a	a	DET
ecletica-204	44	43	whatman	whatman	NOUN
ecletica-204	44	44	fi	fi	NOUN
ecletica-204	44	45	lter	lter	NOUN
ecletica-204	44	46	paper	paper	NOUN
ecletica-204	44	47	no.1	no.1	VERB
ecletica-204	44	48	to	to	PART
ecletica-204	44	49	remove	remove	VERB
ecletica-204	44	50	the	the	DET
ecletica-204	44	51	insoluble	insoluble	ADJ
ecletica-204	44	52	matter	matter	NOUN
ecletica-204	44	53	.	.	PUNCT
ecletica-204	45	1	the	the	DET
ecletica-204	45	2	fi	fi	NOUN
ecletica-204	45	3	lter	lter	NOUN
ecletica-204	45	4	paper	paper	NOUN
ecletica-204	45	5	was	be	AUX
ecletica-204	45	6	washed	wash	VERB
ecletica-204	45	7	with	with	ADP
ecletica-204	45	8	water	water	NOUN
ecletica-204	45	9	and	and	CCONJ
ecletica-204	45	10	the	the	DET
ecletica-204	45	11	washings	washing	NOUN
ecletica-204	45	12	were	be	AUX
ecletica-204	45	13	added	add	VERB
ecletica-204	45	14	to	to	ADP
ecletica-204	45	15	the	the	DET
ecletica-204	45	16	fi	fi	NOUN
ecletica-204	45	17	ltrate	ltrate	NOUN
ecletica-204	45	18	,	,	PUNCT
ecletica-204	45	19	the	the	DET
ecletica-204	45	20	fi	fi	NOUN
ecletica-204	45	21	nal	nal	ADJ
ecletica-204	45	22	volume	volume	NOUN
ecletica-204	45	23	(	(	PUNCT
ecletica-204	45	24	100ml	100ml	NOUN
ecletica-204	45	25	)	)	PUNCT
ecletica-204	45	26	was	be	AUX
ecletica-204	45	27	made	make	VERB
ecletica-204	45	28	with	with	ADP
ecletica-204	45	29	water	water	NOUN
ecletica-204	45	30	.	.	PUNCT
ecletica-204	46	1	a	a	DET
ecletica-204	46	2	suitable	suitable	ADJ
ecletica-204	46	3	aliquot	aliquot	NOUN
ecletica-204	46	4	of	of	ADP
ecletica-204	46	5	this	this	DET
ecletica-204	46	6	solution	solution	NOUN
ecletica-204	46	7	in	in	ADP
ecletica-204	46	8	the	the	DET
ecletica-204	46	9	working	work	VERB
ecletica-204	46	10	range	range	NOUN
ecletica-204	46	11	of	of	ADP
ecletica-204	46	12	sitagliptin	sitagliptin	NOUN
ecletica-204	46	13	phosphate	phosphate	NOUN
ecletica-204	46	14	was	be	AUX
ecletica-204	46	15	treated	treat	VERB
ecletica-204	46	16	as	as	ADP
ecletica-204	46	17	per	per	ADP
ecletica-204	46	18	procedure	procedure	NOUN
ecletica-204	46	19	described	describe	VERB
ecletica-204	46	20	in	in	ADP
ecletica-204	46	21	the	the	DET
ecletica-204	46	22	above	above	ADJ
ecletica-204	46	23	determination	determination	NOUN
ecletica-204	46	24	of	of	ADP
ecletica-204	46	25	pure	pure	ADJ
ecletica-204	46	26	sitagliptin	sitagliptin	NOUN
ecletica-204	46	27	phosphate	phosphate	NOUN
ecletica-204	46	28	.	.	PUNCT
ecletica-204	47	1	the	the	DET
ecletica-204	47	2	nominal	nominal	ADJ
ecletica-204	47	3	content	content	NOUN
ecletica-204	47	4	of	of	ADP
ecletica-204	47	5	stp	stp	PROPN
ecletica-204	47	6	in	in	ADP
ecletica-204	47	7	the	the	DET
ecletica-204	47	8	tablets	tablet	NOUN
ecletica-204	47	9	was	be	AUX
ecletica-204	47	10	calculated	calculate	VERB
ecletica-204	47	11	either	either	CCONJ
ecletica-204	47	12	from	from	ADP
ecletica-204	47	13	a	a	DET
ecletica-204	47	14	previously	previously	ADV
ecletica-204	47	15	plotted	plot	VERB
ecletica-204	47	16	calibration	calibration	NOUN
ecletica-204	47	17	graph	graph	NOUN
ecletica-204	47	18	or	or	CCONJ
ecletica-204	47	19	using	use	VERB
ecletica-204	47	20	the	the	DET
ecletica-204	47	21	regression	regression	NOUN
ecletica-204	47	22	equation	equation	NOUN
ecletica-204	47	23	results	result	NOUN
ecletica-204	47	24	and	and	CCONJ
ecletica-204	47	25	discussion	discussion	NOUN
ecletica-204	47	26	determination	determination	NOUN
ecletica-204	47	27	of	of	ADP
ecletica-204	47	28	absorption	absorption	NOUN
ecletica-204	47	29	maxima	maxima	NOUN
ecletica-204	47	30	(	(	PUNCT
ecletica-204	47	31	λmax	λmax	NOUN
ecletica-204	47	32	):	):	PUNCT
ecletica-204	47	33	to	to	PART
ecletica-204	47	34	determine	determine	VERB
ecletica-204	47	35	the	the	DET
ecletica-204	47	36	λmax	λmax	NOUN
ecletica-204	47	37	10	10	NUM
ecletica-204	47	38	μg	μg	NOUN
ecletica-204	47	39	/	/	SYM
ecletica-204	47	40	ml	ml	PROPN
ecletica-204	47	41	of	of	ADP
ecletica-204	47	42	the	the	DET
ecletica-204	47	43	stp	stp	PROPN
ecletica-204	47	44	was	be	AUX
ecletica-204	47	45	added	add	VERB
ecletica-204	47	46	to	to	ADP
ecletica-204	47	47	10	10	NUM
ecletica-204	47	48	ml	ml	NOUN
ecletica-204	47	49	volumetric	volumetric	NOUN
ecletica-204	47	50	fl	fl	NOUN
ecletica-204	47	51	ask	ask	VERB
ecletica-204	47	52	.	.	PUNCT
ecletica-204	48	1	then	then	ADV
ecletica-204	48	2	1	1	NUM
ecletica-204	48	3	ml	ml	NOUN
ecletica-204	48	4	of	of	ADP
ecletica-204	48	5	8.4	8.4	NUM
ecletica-204	48	6	%	%	NOUN
ecletica-204	48	7	v	v	ADP
ecletica-204	48	8	/	/	SYM
ecletica-204	48	9	v	v	NOUN
ecletica-204	48	10	acetyl	acetyl	NOUN
ecletica-204	48	11	acetone	acetone	NOUN
ecletica-204	48	12	solution	solution	NOUN
ecletica-204	48	13	and	and	CCONJ
ecletica-204	48	14	0.5	0.5	NUM
ecletica-204	48	15	ml	ml	NOUN
ecletica-204	48	16	of	of	ADP
ecletica-204	48	17	20	20	NUM
ecletica-204	48	18	%	%	NOUN
ecletica-204	48	19	formaldehyde	formaldehyde	NOUN
ecletica-204	48	20	reagents	reagent	NOUN
ecletica-204	48	21	were	be	AUX
ecletica-204	48	22	added	add	VERB
ecletica-204	48	23	.	.	PUNCT
ecletica-204	49	1	the	the	DET
ecletica-204	49	2	contents	content	NOUN
ecletica-204	49	3	were	be	AUX
ecletica-204	49	4	mixed	mix	VERB
ecletica-204	49	5	well	well	ADV
ecletica-204	49	6	.	.	PUNCT
ecletica-204	50	1	the	the	DET
ecletica-204	50	2	mixture	mixture	NOUN
ecletica-204	50	3	was	be	AUX
ecletica-204	50	4	heated	heat	VERB
ecletica-204	50	5	for	for	ADP
ecletica-204	50	6	5	5	NUM
ecletica-204	50	7	min	min	NOUN
ecletica-204	50	8	,	,	PUNCT
ecletica-204	50	9	cooled	cool	VERB
ecletica-204	50	10	and	and	CCONJ
ecletica-204	50	11	diluted	dilute	VERB
ecletica-204	50	12	to	to	ADP
ecletica-204	50	13	10	10	NUM
ecletica-204	50	14	ml	ml	NOUN
ecletica-204	50	15	with	with	ADP
ecletica-204	50	16	distilled	distil	VERB
ecletica-204	50	17	water	water	NOUN
ecletica-204	50	18	.	.	PUNCT
ecletica-204	51	1	the	the	DET
ecletica-204	51	2	absorbance	absorbance	NOUN
ecletica-204	51	3	was	be	AUX
ecletica-204	51	4	measured	measure	VERB
ecletica-204	51	5	against	against	ADP
ecletica-204	51	6	reagent	reagent	ADJ
ecletica-204	51	7	blank	blank	NOUN
ecletica-204	51	8	in	in	ADP
ecletica-204	51	9	the	the	DET
ecletica-204	51	10	range	range	NOUN
ecletica-204	51	11	of	of	ADP
ecletica-204	51	12	400	400	NUM
ecletica-204	51	13	-	-	SYM
ecletica-204	51	14	700	700	NUM
ecletica-204	51	15	nm	nm	NOUN
ecletica-204	51	16	.	.	PUNCT
ecletica-204	52	1	λmax	λmax	NOUN
ecletica-204	52	2	for	for	ADP
ecletica-204	52	3	stp	stp	PROPN
ecletica-204	52	4	was	be	AUX
ecletica-204	52	5	found	find	VERB
ecletica-204	52	6	to	to	PART
ecletica-204	52	7	be	be	AUX
ecletica-204	52	8	430	430	NUM
ecletica-204	52	9	nm	nm	NOUN
ecletica-204	52	10	.	.	PUNCT
ecletica-204	53	1	absorption	absorption	NOUN
ecletica-204	53	2	spectrum	spectrum	NOUN
ecletica-204	53	3	of	of	ADP
ecletica-204	53	4	the	the	DET
ecletica-204	53	5	proposed	propose	VERB
ecletica-204	53	6	method	method	NOUN
ecletica-204	53	7	was	be	AUX
ecletica-204	53	8	shown	show	VERB
ecletica-204	53	9	in	in	ADP
ecletica-204	53	10	fig	fig	NOUN
ecletica-204	53	11	.	.	PUNCT
ecletica-204	54	1	2	2	NUM
ecletica-204	54	2	.	.	X
ecletica-204	55	1	under	under	ADP
ecletica-204	55	2	the	the	DET
ecletica-204	55	3	experimental	experimental	ADJ
ecletica-204	55	4	conditions	condition	NOUN
ecletica-204	55	5	each	each	DET
ecletica-204	55	6	reagent	reagent	ADJ
ecletica-204	55	7	blank	blank	NOUN
ecletica-204	55	8	showed	show	VERB
ecletica-204	55	9	a	a	DET
ecletica-204	55	10	negligible	negligible	ADJ
ecletica-204	55	11	absorbance	absorbance	NOUN
ecletica-204	55	12	at	at	ADP
ecletica-204	55	13	the	the	DET
ecletica-204	55	14	corresponding	correspond	VERB
ecletica-204	55	15	λmax	λmax	NOUN
ecletica-204	55	16	.	.	PUNCT
ecletica-204	56	1	fig	fig	NOUN
ecletica-204	57	1	2	2	NUM
ecletica-204	57	2	.	.	PUNCT
ecletica-204	57	3	tentative	tentative	ADJ
ecletica-204	57	4	reaction	reaction	NOUN
ecletica-204	57	5	scheme	scheme	NOUN
ecletica-204	57	6	for	for	ADP
ecletica-204	57	7	the	the	DET
ecletica-204	57	8	formation	formation	NOUN
ecletica-204	57	9	of	of	ADP
ecletica-204	57	10	hantzch	hantzch	ADJ
ecletica-204	57	11	product	product	NOUN
ecletica-204	57	12	chemistry	chemistry	NOUN
ecletica-204	57	13	of	of	ADP
ecletica-204	57	14	the	the	DET
ecletica-204	57	15	colored	colored	ADJ
ecletica-204	57	16	species	specie	NOUN
ecletica-204	57	17	hantzsch	hantzsch	ADJ
ecletica-204	57	18	reaction	reaction	NOUN
ecletica-204	57	19	is	be	AUX
ecletica-204	57	20	a	a	DET
ecletica-204	57	21	known	know	VERB
ecletica-204	57	22	condensation	condensation	NOUN
ecletica-204	57	23	reaction	reaction	NOUN
ecletica-204	57	24	that	that	PRON
ecletica-204	57	25	was	be	AUX
ecletica-204	57	26	reported	report	VERB
ecletica-204	57	27	in	in	ADP
ecletica-204	57	28	the	the	DET
ecletica-204	57	29	literatures	literature	NOUN
ecletica-204	57	30	as	as	ADP
ecletica-204	57	31	a	a	DET
ecletica-204	57	32	useful	useful	ADJ
ecletica-204	57	33	pathway	pathway	NOUN
ecletica-204	57	34	for	for	ADP
ecletica-204	57	35	pyrrole	pyrrole	NOUN
ecletica-204	57	36	and	and	CCONJ
ecletica-204	57	37	pyridine	pyridine	ADJ
ecletica-204	57	38	synthesis	synthesis	NOUN
ecletica-204	57	39	(	(	PUNCT
ecletica-204	57	40	9	9	NUM
ecletica-204	57	41	)	)	PUNCT
ecletica-204	57	42	.	.	PUNCT
ecletica-204	58	1	in	in	ADP
ecletica-204	58	2	the	the	DET
ecletica-204	58	3	same	same	ADJ
ecletica-204	58	4	manner	manner	NOUN
ecletica-204	58	5	,	,	PUNCT
ecletica-204	58	6	acetylacetone	acetylacetone	NOUN
ecletica-204	58	7	together	together	ADV
ecletica-204	58	8	with	with	ADP
ecletica-204	58	9	formaldehyde	formaldehyde	NOUN
ecletica-204	58	10	react	react	NOUN
ecletica-204	58	11	with	with	ADP
ecletica-204	58	12	aliphatic	aliphatic	ADJ
ecletica-204	58	13	amines	amine	NOUN
ecletica-204	58	14	by	by	ADP
ecletica-204	58	15	hantzsch	hantzsch	ADJ
ecletica-204	58	16	reaction	reaction	NOUN
ecletica-204	58	17	forming	form	VERB
ecletica-204	58	18	a	a	DET
ecletica-204	58	19	yellow	yellow	ADJ
ecletica-204	58	20	product	product	NOUN
ecletica-204	58	21	that	that	PRON
ecletica-204	58	22	can	can	AUX
ecletica-204	58	23	be	be	AUX
ecletica-204	58	24	measured	measure	VERB
ecletica-204	58	25	spectrophotometrically	spectrophotometrically	ADV
ecletica-204	58	26	or	or	CCONJ
ecletica-204	58	27	spectrofl	spectrofl	NOUN
ecletica-204	58	28	uorimetrically	uorimetrically	ADV
ecletica-204	58	29	.	.	PUNCT
ecletica-204	59	1	this	this	DET
ecletica-204	59	2	reaction	reaction	NOUN
ecletica-204	59	3	was	be	AUX
ecletica-204	59	4	applied	apply	VERB
ecletica-204	59	5	for	for	ADP
ecletica-204	59	6	the	the	DET
ecletica-204	59	7	determination	determination	NOUN
ecletica-204	59	8	of	of	ADP
ecletica-204	59	9	certain	certain	ADJ
ecletica-204	59	10	sulpha	sulpha	NOUN
ecletica-204	59	11	-	-	PUNCT
ecletica-204	59	12	drug	drug	NOUN
ecletica-204	59	13	(	(	PUNCT
ecletica-204	59	14	10	10	NUM
ecletica-204	59	15	)	)	PUNCT
ecletica-204	59	16	,	,	PUNCT
ecletica-204	59	17	kanamycin	kanamycin	PROPN
ecletica-204	59	18	(	(	PUNCT
ecletica-204	59	19	11	11	NUM
ecletica-204	59	20	)	)	PUNCT
ecletica-204	59	21	,	,	PUNCT
ecletica-204	59	22	lisinopril	lisinopril	NOUN
ecletica-204	59	23	(	(	PUNCT
ecletica-204	59	24	12	12	NUM
ecletica-204	59	25	)	)	PUNCT
ecletica-204	59	26	and	and	CCONJ
ecletica-204	59	27	gabapentin	gabapentin	NOUN
ecletica-204	59	28	and	and	CCONJ
ecletica-204	59	29	cefprozil	cefprozil	PROPN
ecletica-204	59	30	(	(	PUNCT
ecletica-204	59	31	13	13	NUM
ecletica-204	59	32	)	)	PUNCT
ecletica-204	59	33	.	.	PUNCT
ecletica-204	60	1	the	the	DET
ecletica-204	60	2	proposed	propose	VERB
ecletica-204	60	3	method	method	NOUN
ecletica-204	60	4	for	for	ADP
ecletica-204	60	5	determination	determination	NOUN
ecletica-204	60	6	of	of	ADP
ecletica-204	60	7	stp	stp	PROPN
ecletica-204	60	8	(	(	PUNCT
ecletica-204	60	9	primary	primary	ADJ
ecletica-204	60	10	amine	amine	ADJ
ecletica-204	60	11	compound	compound	NOUN
ecletica-204	60	12	)	)	PUNCT
ecletica-204	60	13	was	be	AUX
ecletica-204	60	14	based	base	VERB
ecletica-204	60	15	on	on	ADP
ecletica-204	60	16	hantzsch	hantzsch	ADJ
ecletica-204	60	17	condensation	condensation	NOUN
ecletica-204	60	18	reaction	reaction	NOUN
ecletica-204	60	19	using	use	VERB
ecletica-204	60	20	acetylacetone	acetylacetone	NOUN
ecletica-204	60	21	as	as	ADP
ecletica-204	60	22	β	β	NOUN
ecletica-204	60	23	-diketone	-diketone	PROPN
ecletica-204	60	24	and	and	CCONJ
ecletica-204	60	25	formaldehyde	formaldehyde	NOUN
ecletica-204	60	26	as	as	ADP
ecletica-204	60	27	an	an	DET
ecletica-204	60	28	aldehyde	aldehyde	NOUN
ecletica-204	60	29	to	to	PART
ecletica-204	60	30	form	form	VERB
ecletica-204	60	31	a	a	DET
ecletica-204	60	32	colored	colored	ADJ
ecletica-204	60	33	condensation	condensation	NOUN
ecletica-204	60	34	product	product	NOUN
ecletica-204	60	35	.	.	PUNCT
ecletica-204	61	1	the	the	DET
ecletica-204	61	2	formed	form	VERB
ecletica-204	61	3	yellow	yellow	ADJ
ecletica-204	61	4	color	color	NOUN
ecletica-204	61	5	showed	show	VERB
ecletica-204	61	6	maximum	maximum	ADJ
ecletica-204	61	7	absorption	absorption	NOUN
ecletica-204	61	8	at	at	ADP
ecletica-204	61	9	430	430	NUM
ecletica-204	61	10	nm	nm	NOUN
ecletica-204	61	11	(	(	PUNCT
ecletica-204	61	12	fig	fig	NOUN
ecletica-204	61	13	.	.	PUNCT
ecletica-204	62	1	3	3	NUM
ecletica-204	62	2	)	)	PUNCT
ecletica-204	62	3	.	.	PUNCT
ecletica-204	63	1	the	the	DET
ecletica-204	63	2	probable	probable	ADJ
ecletica-204	63	3	reaction	reaction	NOUN
ecletica-204	63	4	mechanism	mechanism	NOUN
ecletica-204	63	5	was	be	AUX
ecletica-204	63	6	based	base	VERB
ecletica-204	63	7	on	on	ADP
ecletica-204	63	8	the	the	DET
ecletica-204	63	9	reported	report	VERB
ecletica-204	63	10	method	method	NOUN
ecletica-204	63	11	(	(	PUNCT
ecletica-204	63	12	14	14	NUM
ecletica-204	63	13	)	)	PUNCT
ecletica-204	63	14	is	be	AUX
ecletica-204	63	15	given	give	VERB
ecletica-204	63	16	in	in	ADP
ecletica-204	63	17	fig.2	fig.2	PROPN
ecletica-204	63	18	ecl	ecl	PROPN
ecletica-204	63	19	.	.	PROPN
ecletica-204	63	20	quím	quím	PROPN
ecletica-204	63	21	.	.	PUNCT
ecletica-204	64	1	,	,	PUNCT
ecletica-204	64	2	são	são	PROPN
ecletica-204	64	3	paulo	paulo	PROPN
ecletica-204	64	4	,	,	PUNCT
ecletica-204	64	5	35	35	NUM
ecletica-204	64	6	3	3	NUM
ecletica-204	64	7	:	:	PUNCT
ecletica-204	64	8	45	45	NUM
ecletica-204	64	9	53	53	NUM
ecletica-204	64	10	,	,	PUNCT
ecletica-204	64	11	201048	201048	NUM
ecletica-204	64	12	ecl	ecl	PROPN
ecletica-204	64	13	.	.	PROPN
ecletica-204	64	14	quím	quím	PROPN
ecletica-204	64	15	.	.	PUNCT
ecletica-204	64	16	,	,	PUNCT
ecletica-204	64	17	são	são	PROPN
ecletica-204	64	18	paulo	paulo	PROPN
ecletica-204	64	19	,	,	PUNCT
ecletica-204	64	20	35	35	NUM
ecletica-204	64	21	3	3	NUM
ecletica-204	64	22	:	:	PUNCT
ecletica-204	64	23	45	45	NUM
ecletica-204	64	24	53	53	NUM
ecletica-204	64	25	,	,	PUNCT
ecletica-204	64	26	2010	2010	NUM
ecletica-204	64	27	49	49	NUM
ecletica-204	64	28	artigo	artigo	PROPN
ecletica-204	64	29	article	article	NOUN
ecletica-204	64	30	artigo	artigo	PROPN
ecletica-204	64	31	article	article	PROPN
ecletica-204	64	32	fig	fig	VERB
ecletica-204	64	33	3	3	NUM
ecletica-204	64	34	.	.	PUNCT
ecletica-204	65	1	absorption	absorption	NOUN
ecletica-204	65	2	spectra	spectra	NOUN
ecletica-204	65	3	of	of	ADP
ecletica-204	65	4	the	the	DET
ecletica-204	65	5	hantzch	hantzch	ADJ
ecletica-204	65	6	product	product	NOUN
ecletica-204	65	7	0	0	NUM
ecletica-204	65	8	0.2	0.2	NUM
ecletica-204	65	9	0.4	0.4	NUM
ecletica-204	65	10	0.6	0.6	NUM
ecletica-204	65	11	0.8	0.8	NUM
ecletica-204	65	12	1	1	NUM
ecletica-204	65	13	1.2	1.2	NUM
ecletica-204	65	14	390	390	NUM
ecletica-204	65	15	400	400	NUM
ecletica-204	65	16	410	410	NUM
ecletica-204	65	17	420	420	NUM
ecletica-204	65	18	430	430	NUM
ecletica-204	65	19	440	440	NUM
ecletica-204	65	20	450	450	NUM
ecletica-204	65	21	460	460	NUM
ecletica-204	65	22	470	470	NUM
ecletica-204	65	23	480	480	NUM
ecletica-204	65	24	wave	wave	NOUN
ecletica-204	65	25	length	length	NOUN
ecletica-204	65	26	(	(	PUNCT
ecletica-204	65	27	nm	nm	NOUN
ecletica-204	65	28	)	)	PUNCT
ecletica-204	65	29	ab	ab	PROPN
ecletica-204	65	30	so	so	ADV
ecletica-204	65	31	rb	rb	PROPN
ecletica-204	65	32	an	an	DET
ecletica-204	65	33	ce	ce	NOUN
ecletica-204	65	34	investigation	investigation	NOUN
ecletica-204	65	35	of	of	ADP
ecletica-204	65	36	assay	assay	ADJ
ecletica-204	65	37	parameters	parameter	NOUN
ecletica-204	65	38	optimum	optimum	ADJ
ecletica-204	65	39	reagent	reagent	ADJ
ecletica-204	65	40	concentrations	concentration	NOUN
ecletica-204	65	41	required	require	VERB
ecletica-204	65	42	for	for	ADP
ecletica-204	65	43	the	the	DET
ecletica-204	65	44	formation	formation	NOUN
ecletica-204	65	45	of	of	ADP
ecletica-204	65	46	sensitive	sensitive	ADJ
ecletica-204	65	47	and	and	CCONJ
ecletica-204	65	48	quantitative	quantitative	ADJ
ecletica-204	65	49	colored	colored	ADJ
ecletica-204	65	50	products	product	NOUN
ecletica-204	65	51	were	be	AUX
ecletica-204	65	52	determined	determine	VERB
ecletica-204	65	53	by	by	ADP
ecletica-204	65	54	varying	vary	VERB
ecletica-204	65	55	one	one	NUM
ecletica-204	65	56	reagent	reagent	ADJ
ecletica-204	65	57	concentration	concentration	NOUN
ecletica-204	65	58	and	and	CCONJ
ecletica-204	65	59	fi	fi	NOUN
ecletica-204	65	60	xing	xe	VERB
ecletica-204	65	61	the	the	DET
ecletica-204	65	62	concentrations	concentration	NOUN
ecletica-204	65	63	of	of	ADP
ecletica-204	65	64	other	other	ADJ
ecletica-204	65	65	reagents	reagent	NOUN
ecletica-204	65	66	and	and	CCONJ
ecletica-204	65	67	its	its	PRON
ecletica-204	65	68	effect	effect	NOUN
ecletica-204	65	69	on	on	ADP
ecletica-204	65	70	absorbance	absorbance	NOUN
ecletica-204	65	71	was	be	AUX
ecletica-204	65	72	measured	measure	VERB
ecletica-204	65	73	at	at	ADP
ecletica-204	65	74	430	430	NUM
ecletica-204	65	75	nm	nm	NOUN
ecletica-204	65	76	.	.	PUNCT
ecletica-204	66	1	effect	effect	NOUN
ecletica-204	66	2	of	of	ADP
ecletica-204	66	3	heating	heating	NOUN
ecletica-204	66	4	time	time	NOUN
ecletica-204	66	5	:	:	PUNCT
ecletica-204	66	6	to	to	PART
ecletica-204	66	7	study	study	VERB
ecletica-204	66	8	the	the	DET
ecletica-204	66	9	effect	effect	NOUN
ecletica-204	66	10	of	of	ADP
ecletica-204	66	11	heating	heating	NOUN
ecletica-204	66	12	time	time	NOUN
ecletica-204	66	13	for	for	ADP
ecletica-204	66	14	the	the	DET
ecletica-204	66	15	development	development	NOUN
ecletica-204	66	16	of	of	ADP
ecletica-204	66	17	maximum	maximum	ADJ
ecletica-204	66	18	color	color	NOUN
ecletica-204	66	19	,	,	PUNCT
ecletica-204	66	20	the	the	DET
ecletica-204	66	21	contents	content	NOUN
ecletica-204	66	22	of	of	ADP
ecletica-204	66	23	the	the	DET
ecletica-204	66	24	mixture	mixture	NOUN
ecletica-204	66	25	were	be	AUX
ecletica-204	66	26	heated	heat	VERB
ecletica-204	66	27	for	for	ADP
ecletica-204	66	28	up	up	ADP
ecletica-204	66	29	to	to	PART
ecletica-204	66	30	30	30	NUM
ecletica-204	66	31	min	min	NOUN
ecletica-204	66	32	at	at	ADP
ecletica-204	66	33	100	100	NUM
ecletica-204	66	34	±	±	NUM
ecletica-204	66	35	1	1	NUM
ecletica-204	66	36	°	°	NOUN
ecletica-204	66	37	c	c	NOUN
ecletica-204	66	38	.	.	PUNCT
ecletica-204	67	1	the	the	DET
ecletica-204	67	2	intensity	intensity	NOUN
ecletica-204	67	3	of	of	ADP
ecletica-204	67	4	the	the	DET
ecletica-204	67	5	color	color	NOUN
ecletica-204	67	6	developed	develop	VERB
ecletica-204	67	7	was	be	AUX
ecletica-204	67	8	measured	measure	VERB
ecletica-204	67	9	at	at	ADP
ecletica-204	67	10	room	room	NOUN
ecletica-204	67	11	temperature	temperature	NOUN
ecletica-204	67	12	(	(	PUNCT
ecletica-204	67	13	25	25	NUM
ecletica-204	67	14	±	±	NUM
ecletica-204	67	15	1	1	NUM
ecletica-204	67	16	°	°	ADP
ecletica-204	67	17	c	c	NOUN
ecletica-204	67	18	)	)	PUNCT
ecletica-204	67	19	after	after	ADP
ecletica-204	67	20	dilution	dilution	NOUN
ecletica-204	67	21	to	to	ADP
ecletica-204	67	22	10.0ml	10.0ml	NUM
ecletica-204	67	23	with	with	ADP
ecletica-204	67	24	double	double	ADJ
ecletica-204	67	25	distilled	distil	VERB
ecletica-204	67	26	water	water	NOUN
ecletica-204	67	27	.	.	PUNCT
ecletica-204	68	1	it	it	PRON
ecletica-204	68	2	is	be	AUX
ecletica-204	68	3	apparent	apparent	ADJ
ecletica-204	68	4	from	from	ADP
ecletica-204	68	5	this	this	DET
ecletica-204	68	6	investigation	investigation	NOUN
ecletica-204	68	7	that	that	SCONJ
ecletica-204	68	8	the	the	DET
ecletica-204	68	9	maximum	maximum	ADJ
ecletica-204	68	10	intensity	intensity	NOUN
ecletica-204	68	11	of	of	ADP
ecletica-204	68	12	color	color	NOUN
ecletica-204	68	13	was	be	AUX
ecletica-204	68	14	obtained	obtain	VERB
ecletica-204	68	15	after	after	ADP
ecletica-204	68	16	5	5	NUM
ecletica-204	68	17	min	min	NOUN
ecletica-204	68	18	of	of	ADP
ecletica-204	68	19	heating	heating	NOUN
ecletica-204	68	20	and	and	CCONJ
ecletica-204	68	21	remained	remain	VERB
ecletica-204	68	22	constant	constant	ADJ
ecletica-204	68	23	up	up	ADP
ecletica-204	68	24	to	to	PART
ecletica-204	68	25	30	30	NUM
ecletica-204	68	26	min	min	NOUN
ecletica-204	68	27	.	.	PROPN
ecletica-204	69	1	therefore	therefore	ADV
ecletica-204	69	2	,	,	PUNCT
ecletica-204	69	3	the	the	DET
ecletica-204	69	4	optimum	optimum	ADJ
ecletica-204	69	5	heating	heating	NOUN
ecletica-204	69	6	time	time	NOUN
ecletica-204	69	7	was	be	AUX
ecletica-204	69	8	fi	fi	NOUN
ecletica-204	69	9	xed	xe	VERB
ecletica-204	69	10	at	at	ADP
ecletica-204	69	11	5	5	NUM
ecletica-204	69	12	min	min	NOUN
ecletica-204	69	13	.	.	PROPN
ecletica-204	69	14	effect	effect	NOUN
ecletica-204	69	15	of	of	ADP
ecletica-204	69	16	reagent	reagent	ADJ
ecletica-204	69	17	concentration	concentration	NOUN
ecletica-204	69	18	:	:	PUNCT
ecletica-204	69	19	the	the	DET
ecletica-204	69	20	effect	effect	NOUN
ecletica-204	69	21	of	of	ADP
ecletica-204	69	22	acetyl	acetyl	NOUN
ecletica-204	69	23	acetone	acetone	NOUN
ecletica-204	69	24	and	and	CCONJ
ecletica-204	69	25	formaldehyde	formaldehyde	NOUN
ecletica-204	69	26	concentration	concentration	NOUN
ecletica-204	69	27	on	on	ADP
ecletica-204	69	28	the	the	DET
ecletica-204	69	29	absorbance	absorbance	NOUN
ecletica-204	69	30	was	be	AUX
ecletica-204	69	31	studied	study	VERB
ecletica-204	69	32	;	;	PUNCT
ecletica-204	69	33	volumes	volume	NOUN
ecletica-204	69	34	from	from	ADP
ecletica-204	69	35	0.5	0.5	NUM
ecletica-204	69	36	-	-	SYM
ecletica-204	69	37	2.5ml	2.5ml	NUM
ecletica-204	69	38	of	of	ADP
ecletica-204	69	39	8.4	8.4	NUM
ecletica-204	69	40	%	%	NOUN
ecletica-204	69	41	acetyl	acetyl	NOUN
ecletica-204	69	42	acetone	acetone	NOUN
ecletica-204	69	43	solutions	solution	NOUN
ecletica-204	69	44	and	and	CCONJ
ecletica-204	69	45	0.1	0.1	NUM
ecletica-204	69	46	to	to	ADP
ecletica-204	69	47	1.0ml	1.0ml	NUM
ecletica-204	69	48	of	of	ADP
ecletica-204	69	49	20	20	NUM
ecletica-204	69	50	%	%	NOUN
ecletica-204	69	51	formaldehyde	formaldehyde	NOUN
ecletica-204	69	52	solutions	solution	NOUN
ecletica-204	69	53	were	be	AUX
ecletica-204	69	54	examined	examine	VERB
ecletica-204	69	55	.	.	PUNCT
ecletica-204	70	1	the	the	DET
ecletica-204	70	2	investigations	investigation	NOUN
ecletica-204	70	3	showed	show	VERB
ecletica-204	70	4	that	that	SCONJ
ecletica-204	70	5	1ml	1ml	NOUN
ecletica-204	70	6	of	of	ADP
ecletica-204	70	7	acetyl	acetyl	NOUN
ecletica-204	70	8	acetone	acetone	NOUN
ecletica-204	70	9	and	and	CCONJ
ecletica-204	70	10	0.5ml	0.5ml	PROPN
ecletica-204	70	11	of	of	ADP
ecletica-204	70	12	formaldehyde	formaldehyde	NOUN
ecletica-204	70	13	gave	give	VERB
ecletica-204	70	14	maximum	maximum	ADJ
ecletica-204	70	15	absorbance	absorbance	NOUN
ecletica-204	70	16	.	.	PUNCT
ecletica-204	71	1	so	so	ADV
ecletica-204	71	2	the	the	DET
ecletica-204	71	3	same	same	ADJ
ecletica-204	71	4	volumes	volume	NOUN
ecletica-204	71	5	of	of	ADP
ecletica-204	71	6	both	both	CCONJ
ecletica-204	71	7	the	the	DET
ecletica-204	71	8	reagents	reagent	NOUN
ecletica-204	71	9	were	be	AUX
ecletica-204	71	10	chosen	choose	VERB
ecletica-204	71	11	for	for	ADP
ecletica-204	71	12	the	the	DET
ecletica-204	71	13	procedure	procedure	NOUN
ecletica-204	71	14	.	.	PUNCT
ecletica-204	72	1	effect	effect	NOUN
ecletica-204	72	2	of	of	ADP
ecletica-204	72	3	ph	ph	ADJ
ecletica-204	72	4	:	:	PUNCT
ecletica-204	72	5	different	different	ADJ
ecletica-204	72	6	acetate	acetate	NOUN
ecletica-204	72	7	buffers	buffer	NOUN
ecletica-204	72	8	with	with	ADP
ecletica-204	72	9	ph	ph	ADJ
ecletica-204	72	10	range	range	NOUN
ecletica-204	72	11	of	of	ADP
ecletica-204	72	12	3.0	3.0	NUM
ecletica-204	72	13	7.0	7.0	NUM
ecletica-204	72	14	were	be	AUX
ecletica-204	72	15	tried	try	VERB
ecletica-204	72	16	and	and	CCONJ
ecletica-204	72	17	ph	ph	VERB
ecletica-204	72	18	5	5	NUM
ecletica-204	72	19	was	be	AUX
ecletica-204	72	20	the	the	DET
ecletica-204	72	21	ph	ph	NOUN
ecletica-204	72	22	of	of	ADP
ecletica-204	72	23	choice	choice	NOUN
ecletica-204	72	24	for	for	ADP
ecletica-204	72	25	the	the	DET
ecletica-204	72	26	proposed	propose	VERB
ecletica-204	72	27	method	method	NOUN
ecletica-204	72	28	.	.	PUNCT
ecletica-204	73	1	effect	effect	NOUN
ecletica-204	73	2	of	of	ADP
ecletica-204	73	3	solvents	solvent	NOUN
ecletica-204	73	4	:	:	PUNCT
ecletica-204	73	5	different	different	ADJ
ecletica-204	73	6	diluting	dilute	VERB
ecletica-204	73	7	solvents	solvent	NOUN
ecletica-204	73	8	were	be	AUX
ecletica-204	73	9	used	use	VERB
ecletica-204	73	10	,	,	PUNCT
ecletica-204	73	11	such	such	ADJ
ecletica-204	73	12	as	as	ADP
ecletica-204	73	13	water	water	NOUN
ecletica-204	73	14	,	,	PUNCT
ecletica-204	73	15	ethanol	ethanol	NOUN
ecletica-204	73	16	,	,	PUNCT
ecletica-204	73	17	methanol	methanol	NOUN
ecletica-204	73	18	,	,	PUNCT
ecletica-204	73	19	acetonitrile	acetonitrile	NOUN
ecletica-204	73	20	and	and	CCONJ
ecletica-204	73	21	acetone	acetone	NOUN
ecletica-204	73	22	.	.	PUNCT
ecletica-204	74	1	best	good	ADJ
ecletica-204	74	2	color	color	NOUN
ecletica-204	74	3	intensities	intensity	NOUN
ecletica-204	74	4	were	be	AUX
ecletica-204	74	5	obtained	obtain	VERB
ecletica-204	74	6	using	use	VERB
ecletica-204	74	7	the	the	DET
ecletica-204	74	8	fi	fi	NOUN
ecletica-204	74	9	rst	rst	PROPN
ecletica-204	74	10	three	three	NUM
ecletica-204	74	11	solvents	solvent	NOUN
ecletica-204	74	12	;	;	PUNCT
ecletica-204	74	13	water	water	NOUN
ecletica-204	74	14	was	be	AUX
ecletica-204	74	15	used	use	VERB
ecletica-204	74	16	,	,	PUNCT
ecletica-204	74	17	being	be	AUX
ecletica-204	74	18	the	the	DET
ecletica-204	74	19	most	most	ADV
ecletica-204	74	20	available	available	ADJ
ecletica-204	74	21	solvent	solvent	NOUN
ecletica-204	74	22	.	.	PUNCT
ecletica-204	75	1	interference	interference	NOUN
ecletica-204	75	2	studies	study	NOUN
ecletica-204	75	3	to	to	PART
ecletica-204	75	4	study	study	VERB
ecletica-204	75	5	the	the	DET
ecletica-204	75	6	potential	potential	ADJ
ecletica-204	75	7	interference	interference	NOUN
ecletica-204	75	8	from	from	ADP
ecletica-204	75	9	the	the	DET
ecletica-204	75	10	commonly	commonly	ADV
ecletica-204	75	11	used	use	VERB
ecletica-204	75	12	excipients	excipient	NOUN
ecletica-204	75	13	and	and	CCONJ
ecletica-204	75	14	other	other	ADJ
ecletica-204	75	15	additives	additive	NOUN
ecletica-204	75	16	such	such	ADJ
ecletica-204	75	17	as	as	ADP
ecletica-204	75	18	glucose	glucose	NOUN
ecletica-204	75	19	,	,	PUNCT
ecletica-204	75	20	lactose	lactose	NOUN
ecletica-204	75	21	,	,	PUNCT
ecletica-204	75	22	starch	starch	NOUN
ecletica-204	75	23	,	,	PUNCT
ecletica-204	75	24	sodium	sodium	NOUN
ecletica-204	75	25	starch	starch	NOUN
ecletica-204	75	26	glycolate	glycolate	NOUN
ecletica-204	75	27	,	,	PUNCT
ecletica-204	75	28	cellulose	cellulose	NOUN
ecletica-204	75	29	,	,	PUNCT
ecletica-204	75	30	magnesium	magnesium	NOUN
ecletica-204	75	31	stearate	stearate	NOUN
ecletica-204	75	32	and	and	CCONJ
ecletica-204	75	33	ascorbic	ascorbic	NOUN
ecletica-204	75	34	acid	acid	NOUN
ecletica-204	75	35	,	,	PUNCT
ecletica-204	75	36	recovery	recovery	NOUN
ecletica-204	75	37	studies	study	NOUN
ecletica-204	75	38	were	be	AUX
ecletica-204	75	39	carried	carry	VERB
ecletica-204	75	40	out	out	ADP
ecletica-204	75	41	.	.	PUNCT
ecletica-204	76	1	under	under	ADP
ecletica-204	76	2	the	the	DET
ecletica-204	76	3	experimental	experimental	ADJ
ecletica-204	76	4	conditions	condition	NOUN
ecletica-204	76	5	employed	employ	VERB
ecletica-204	76	6	,	,	PUNCT
ecletica-204	76	7	to	to	ADP
ecletica-204	76	8	a	a	DET
ecletica-204	76	9	known	know	VERB
ecletica-204	76	10	amount	amount	NOUN
ecletica-204	76	11	of	of	ADP
ecletica-204	76	12	drug	drug	NOUN
ecletica-204	76	13	(	(	PUNCT
ecletica-204	76	14	sitagliptin	sitagliptin	NOUN
ecletica-204	76	15	phosphate	phosphate	NOUN
ecletica-204	76	16	25	25	NUM
ecletica-204	76	17	μg	μg	NOUN
ecletica-204	76	18	/	/	SYM
ecletica-204	76	19	ml	ml	NOUN
ecletica-204	76	20	)	)	PUNCT
ecletica-204	76	21	,	,	PUNCT
ecletica-204	76	22	excipients	excipient	NOUN
ecletica-204	76	23	in	in	ADP
ecletica-204	76	24	different	different	ADJ
ecletica-204	76	25	concentrations	concentration	NOUN
ecletica-204	76	26	were	be	AUX
ecletica-204	76	27	added	add	VERB
ecletica-204	76	28	and	and	CCONJ
ecletica-204	76	29	analyzed	analyze	VERB
ecletica-204	76	30	.	.	PUNCT
ecletica-204	77	1	results	result	NOUN
ecletica-204	77	2	of	of	ADP
ecletica-204	77	3	the	the	DET
ecletica-204	77	4	recovery	recovery	NOUN
ecletica-204	77	5	analysis	analysis	NOUN
ecletica-204	77	6	are	be	AUX
ecletica-204	77	7	presented	present	VERB
ecletica-204	77	8	in	in	ADP
ecletica-204	77	9	table	table	NOUN
ecletica-204	77	10	1	1	NUM
ecletica-204	77	11	.	.	PUNCT
ecletica-204	78	1	excipients	excipient	NOUN
ecletica-204	78	2	at	at	ADP
ecletica-204	78	3	the	the	DET
ecletica-204	78	4	concentrations	concentration	NOUN
ecletica-204	78	5	shown	show	VERB
ecletica-204	78	6	in	in	ADP
ecletica-204	78	7	table	table	NOUN
ecletica-204	78	8	1	1	NUM
ecletica-204	78	9	do	do	AUX
ecletica-204	78	10	not	not	PART
ecletica-204	78	11	interfere	interfere	VERB
ecletica-204	78	12	with	with	ADP
ecletica-204	78	13	the	the	DET
ecletica-204	78	14	assay	assay	NOUN
ecletica-204	78	15	.	.	PUNCT
ecletica-204	79	1	in	in	ADP
ecletica-204	79	2	addition	addition	NOUN
ecletica-204	79	3	recoveries	recovery	NOUN
ecletica-204	79	4	in	in	ADP
ecletica-204	79	5	most	most	ADJ
ecletica-204	79	6	cases	case	NOUN
ecletica-204	79	7	were	be	AUX
ecletica-204	79	8	around	around	ADV
ecletica-204	79	9	100	100	NUM
ecletica-204	79	10	%	%	NOUN
ecletica-204	79	11	and	and	CCONJ
ecletica-204	79	12	the	the	DET
ecletica-204	79	13	lower	low	ADJ
ecletica-204	79	14	relative	relative	ADJ
ecletica-204	79	15	standard	standard	ADJ
ecletica-204	79	16	deviation	deviation	NOUN
ecletica-204	79	17	(	(	PUNCT
ecletica-204	79	18	rsd	rsd	NOUN
ecletica-204	79	19	)	)	PUNCT
ecletica-204	79	20	values	value	NOUN
ecletica-204	79	21	indicate	indicate	VERB
ecletica-204	79	22	the	the	DET
ecletica-204	79	23	good	good	ADJ
ecletica-204	79	24	precision	precision	NOUN
ecletica-204	79	25	of	of	ADP
ecletica-204	79	26	the	the	DET
ecletica-204	79	27	proposed	propose	VERB
ecletica-204	79	28	method	method	NOUN
ecletica-204	79	29	.	.	PUNCT
ecletica-204	80	1	table	table	NOUN
ecletica-204	80	2	1	1	NUM
ecletica-204	80	3	.	.	PUNCT
ecletica-204	81	1	determination	determination	NOUN
ecletica-204	81	2	of	of	ADP
ecletica-204	81	3	stp	stp	PROPN
ecletica-204	81	4	in	in	ADP
ecletica-204	81	5	the	the	DET
ecletica-204	81	6	presence	presence	NOUN
ecletica-204	81	7	of	of	ADP
ecletica-204	81	8	excipients	excipient	NOUN
ecletica-204	81	9	s.no	s.no	NOUN
ecletica-204	81	10	.	.	PUNCT
ecletica-204	81	11	excipients	excipient	NOUN
ecletica-204	81	12	amount	amount	NOUN
ecletica-204	81	13	taken	take	VERB
ecletica-204	81	14	(	(	PUNCT
ecletica-204	81	15	25	25	NUM
ecletica-204	81	16	μg	μg	NOUN
ecletica-204	81	17	/	/	SYM
ecletica-204	81	18	ml	ml	NOUN
ecletica-204	81	19	)	)	PUNCT
ecletica-204	81	20	recovery	recovery	NOUN
ecletica-204	81	21	(	(	PUNCT
ecletica-204	81	22	%	%	INTJ
ecletica-204	81	23	)	)	PUNCT
ecletica-204	81	24	rsd	rsd	NOUN
ecletica-204	81	25	(	(	PUNCT
ecletica-204	81	26	%	%	NOUN
ecletica-204	81	27	)	)	PUNCT
ecletica-204	81	28	(	(	PUNCT
ecletica-204	81	29	n	n	NOUN
ecletica-204	81	30	=	=	SYM
ecletica-204	81	31	5	5	NUM
ecletica-204	81	32	)	)	PUNCT
ecletica-204	81	33	1	1	NUM
ecletica-204	81	34	cellulose	cellulose	NOUN
ecletica-204	81	35	300	300	NUM
ecletica-204	81	36	99.8	99.8	NUM
ecletica-204	81	37	0.26	0.26	NUM
ecletica-204	81	38	2	2	NUM
ecletica-204	81	39	glucose	glucose	NOUN
ecletica-204	81	40	50	50	NUM
ecletica-204	81	41	99.6	99.6	NUM
ecletica-204	81	42	0.15	0.15	NUM
ecletica-204	81	43	3	3	NUM
ecletica-204	81	44	lactose	lactose	NOUN
ecletica-204	81	45	300	300	NUM
ecletica-204	81	46	99.4	99.4	NUM
ecletica-204	81	47	0.36	0.36	NUM
ecletica-204	81	48	4	4	NUM
ecletica-204	81	49	starch	starch	NOUN
ecletica-204	81	50	200	200	NUM
ecletica-204	81	51	100.2	100.2	NUM
ecletica-204	81	52	0.42	0.42	NUM
ecletica-204	81	53	5	5	NUM
ecletica-204	81	54	sodium	sodium	NOUN
ecletica-204	81	55	starch	starch	NOUN
ecletica-204	81	56	glycolate	glycolate	VERB
ecletica-204	81	57	100	100	NUM
ecletica-204	81	58	99.8	99.8	NUM
ecletica-204	81	59	0.28	0.28	NUM
ecletica-204	81	60	6	6	NUM
ecletica-204	81	61	magnesium	magnesium	NOUN
ecletica-204	81	62	stearate	stearate	NOUN
ecletica-204	81	63	50	50	NUM
ecletica-204	81	64	99.5	99.5	NUM
ecletica-204	81	65	0.37	0.37	NUM
ecletica-204	81	66	7	7	NUM
ecletica-204	81	67	ascorbic	ascorbic	NOUN
ecletica-204	81	68	acid	acid	NOUN
ecletica-204	81	69	50	50	NUM
ecletica-204	81	70	100.1	100.1	NUM
ecletica-204	81	71	0.46	0.46	NUM
ecletica-204	81	72	validation	validation	NOUN
ecletica-204	81	73	of	of	ADP
ecletica-204	81	74	the	the	DET
ecletica-204	81	75	method	method	NOUN
ecletica-204	81	76	:	:	PUNCT
ecletica-204	81	77	detection	detection	NOUN
ecletica-204	81	78	and	and	CCONJ
ecletica-204	81	79	quantifi	quantifi	ADJ
ecletica-204	81	80	cation	cation	NOUN
ecletica-204	81	81	limits	limit	NOUN
ecletica-204	81	82	:	:	PUNCT
ecletica-204	81	83	according	accord	VERB
ecletica-204	81	84	to	to	ADP
ecletica-204	81	85	the	the	DET
ecletica-204	81	86	analytical	analytical	ADJ
ecletica-204	81	87	methods	method	NOUN
ecletica-204	81	88	committee(15	committee(15	NOUN
ecletica-204	81	89	)	)	PUNCT
ecletica-204	81	90	the	the	DET
ecletica-204	81	91	detection	detection	NOUN
ecletica-204	81	92	limit	limit	NOUN
ecletica-204	81	93	(	(	PUNCT
ecletica-204	81	94	lod	lod	PROPN
ecletica-204	81	95	)	)	PUNCT
ecletica-204	81	96	is	be	AUX
ecletica-204	81	97	the	the	DET
ecletica-204	81	98	concentration	concentration	NOUN
ecletica-204	81	99	of	of	ADP
ecletica-204	81	100	drug	drug	NOUN
ecletica-204	81	101	corresponding	correspond	VERB
ecletica-204	81	102	to	to	ADP
ecletica-204	81	103	a	a	DET
ecletica-204	81	104	signal	signal	NOUN
ecletica-204	81	105	equal	equal	ADJ
ecletica-204	81	106	to	to	ADP
ecletica-204	81	107	the	the	DET
ecletica-204	81	108	blank	blank	ADJ
ecletica-204	81	109	mean	mean	NOUN
ecletica-204	81	110	(	(	PUNCT
ecletica-204	81	111	yb	yb	PROPN
ecletica-204	81	112	)	)	PUNCT
ecletica-204	81	113	plus	plus	CCONJ
ecletica-204	81	114	three	three	NUM
ecletica-204	81	115	times	time	NOUN
ecletica-204	81	116	the	the	DET
ecletica-204	81	117	standard	standard	ADJ
ecletica-204	81	118	deviation	deviation	NOUN
ecletica-204	81	119	of	of	ADP
ecletica-204	81	120	the	the	DET
ecletica-204	81	121	blank	blank	ADJ
ecletica-204	81	122	(	(	PUNCT
ecletica-204	81	123	sb	sb	NOUN
ecletica-204	81	124	)	)	PUNCT
ecletica-204	81	125	.	.	PUNCT
ecletica-204	82	1	quantifi	quantifi	PROPN
ecletica-204	82	2	cation	cation	NOUN
ecletica-204	82	3	limit	limit	NOUN
ecletica-204	82	4	(	(	PUNCT
ecletica-204	82	5	loq	loq	PROPN
ecletica-204	82	6	)	)	PUNCT
ecletica-204	82	7	is	be	AUX
ecletica-204	82	8	the	the	DET
ecletica-204	82	9	concentration	concentration	NOUN
ecletica-204	82	10	of	of	ADP
ecletica-204	82	11	drug	drug	NOUN
ecletica-204	82	12	corresponding	correspond	VERB
ecletica-204	82	13	to	to	ADP
ecletica-204	82	14	the	the	DET
ecletica-204	82	15	blank	blank	ADJ
ecletica-204	82	16	mean	mean	NOUN
ecletica-204	82	17	plus	plus	CCONJ
ecletica-204	82	18	ten	ten	NUM
ecletica-204	82	19	times	time	NOUN
ecletica-204	82	20	the	the	DET
ecletica-204	82	21	standard	standard	ADJ
ecletica-204	82	22	deviation	deviation	NOUN
ecletica-204	82	23	of	of	ADP
ecletica-204	82	24	the	the	DET
ecletica-204	82	25	blank	blank	NOUN
ecletica-204	82	26	.	.	PUNCT
ecletica-204	83	1	the	the	DET
ecletica-204	83	2	lod	lod	PROPN
ecletica-204	83	3	and	and	CCONJ
ecletica-204	83	4	loq	loq	PROPN
ecletica-204	83	5	values	value	NOUN
ecletica-204	83	6	for	for	ADP
ecletica-204	83	7	stp	stp	PROPN
ecletica-204	83	8	were	be	AUX
ecletica-204	83	9	found	find	VERB
ecletica-204	83	10	to	to	PART
ecletica-204	83	11	be	be	AUX
ecletica-204	83	12	1.947	1.947	NUM
ecletica-204	83	13	and	and	CCONJ
ecletica-204	83	14	5.90	5.90	NUM
ecletica-204	83	15	μg	μg	NOUN
ecletica-204	83	16	/ml	/ml	PUNCT
ecletica-204	83	17	respectively	respectively	ADV
ecletica-204	83	18	.	.	PUNCT
ecletica-204	84	1	quantifi	quantifi	PROPN
ecletica-204	84	2	cation	cation	NOUN
ecletica-204	84	3	:	:	PUNCT
ecletica-204	84	4	the	the	DET
ecletica-204	84	5	optical	optical	ADJ
ecletica-204	84	6	characteristics	characteristic	NOUN
ecletica-204	84	7	such	such	ADJ
ecletica-204	84	8	as	as	ADP
ecletica-204	84	9	beer	beer	NOUN
ecletica-204	84	10	’s	’s	PART
ecletica-204	84	11	law	law	NOUN
ecletica-204	84	12	limits	limit	NOUN
ecletica-204	84	13	(	(	PUNCT
ecletica-204	84	14	fig	fig	NOUN
ecletica-204	84	15	:	:	PUNCT
ecletica-204	84	16	4	4	NUM
ecletica-204	84	17	)	)	PUNCT
ecletica-204	84	18	,	,	PUNCT
ecletica-204	84	19	sandell	sandell	NOUN
ecletica-204	84	20	’s	’s	PART
ecletica-204	84	21	sensitivity	sensitivity	NOUN
ecletica-204	84	22	and	and	CCONJ
ecletica-204	84	23	molar	molar	ADJ
ecletica-204	84	24	absorptivity	absorptivity	NOUN
ecletica-204	84	25	were	be	AUX
ecletica-204	84	26	calculated	calculate	VERB
ecletica-204	84	27	for	for	ADP
ecletica-204	84	28	the	the	DET
ecletica-204	84	29	proposed	propose	VERB
ecletica-204	84	30	method	method	NOUN
ecletica-204	84	31	and	and	CCONJ
ecletica-204	84	32	the	the	DET
ecletica-204	84	33	results	result	NOUN
ecletica-204	84	34	are	be	AUX
ecletica-204	84	35	summarized	summarize	VERB
ecletica-204	84	36	in	in	ADP
ecletica-204	84	37	table	table	NOUN
ecletica-204	84	38	2	2	NUM
ecletica-204	84	39	.	.	PUNCT
ecletica-204	85	1	regression	regression	VERB
ecletica-204	85	2	analysis	analysis	NOUN
ecletica-204	85	3	of	of	ADP
ecletica-204	85	4	the	the	DET
ecletica-204	85	5	beer	beer	NOUN
ecletica-204	85	6	’s	’s	PART
ecletica-204	85	7	law	law	NOUN
ecletica-204	85	8	plot	plot	NOUN
ecletica-204	85	9	at	at	ADP
ecletica-204	85	10	their	their	PRON
ecletica-204	85	11	λmax	λmax	NOUN
ecletica-204	85	12	revealed	reveal	VERB
ecletica-204	85	13	a	a	DET
ecletica-204	85	14	good	good	ADJ
ecletica-204	85	15	correlation	correlation	NOUN
ecletica-204	85	16	.	.	PUNCT
ecletica-204	86	1	graphs	graph	NOUN
ecletica-204	86	2	of	of	ADP
ecletica-204	86	3	absorbance	absorbance	NOUN
ecletica-204	86	4	versus	versus	ADP
ecletica-204	86	5	concentration	concentration	NOUN
ecletica-204	86	6	showed	show	VERB
ecletica-204	86	7	zero	zero	NUM
ecletica-204	86	8	intercept	intercept	NOUN
ecletica-204	86	9	and	and	CCONJ
ecletica-204	86	10	are	be	AUX
ecletica-204	86	11	described	describe	VERB
ecletica-204	86	12	by	by	ADP
ecletica-204	86	13	the	the	DET
ecletica-204	86	14	regression	regression	NOUN
ecletica-204	86	15	equation	equation	NOUN
ecletica-204	86	16	y	y	PROPN
ecletica-204	86	17	=	=	PUNCT
ecletica-204	86	18	bx	bx	PROPN
ecletica-204	86	19	+	+	CCONJ
ecletica-204	86	20	a	a	PRON
ecletica-204	86	21	(	(	PUNCT
ecletica-204	86	22	where	where	SCONJ
ecletica-204	86	23	y	y	PROPN
ecletica-204	86	24	is	be	AUX
ecletica-204	86	25	the	the	DET
ecletica-204	86	26	absorbance	absorbance	NOUN
ecletica-204	86	27	,	,	PUNCT
ecletica-204	86	28	b	b	PROPN
ecletica-204	86	29	is	be	AUX
ecletica-204	86	30	the	the	DET
ecletica-204	86	31	slope	slope	NOUN
ecletica-204	86	32	,	,	PUNCT
ecletica-204	86	33	x	x	X
ecletica-204	86	34	is	be	AUX
ecletica-204	86	35	the	the	DET
ecletica-204	86	36	concentration	concentration	NOUN
ecletica-204	86	37	of	of	ADP
ecletica-204	86	38	drug	drug	NOUN
ecletica-204	86	39	in	in	ADP
ecletica-204	86	40	μg	μg	PROPN
ecletica-204	86	41	/ml	/ml	PUNCT
ecletica-204	86	42	and	and	CCONJ
ecletica-204	86	43	a	a	PRON
ecletica-204	86	44	is	be	AUX
ecletica-204	86	45	the	the	DET
ecletica-204	86	46	intercept	intercept	NOUN
ecletica-204	86	47	)	)	PUNCT
ecletica-204	86	48	obtained	obtain	VERB
ecletica-204	86	49	by	by	ADP
ecletica-204	86	50	least	least	ADJ
ecletica-204	86	51	squares	square	NOUN
ecletica-204	86	52	method	method	NOUN
ecletica-204	86	53	.	.	PUNCT
ecletica-204	87	1	the	the	DET
ecletica-204	87	2	results	result	NOUN
ecletica-204	87	3	were	be	AUX
ecletica-204	87	4	summarized	summarize	VERB
ecletica-204	87	5	in	in	ADP
ecletica-204	87	6	table	table	NOUN
ecletica-204	87	7	2	2	NUM
ecletica-204	87	8	.	.	PUNCT
ecletica-204	88	1	ecl	ecl	PROPN
ecletica-204	88	2	.	.	PROPN
ecletica-204	88	3	quím	quím	PROPN
ecletica-204	88	4	.	.	PUNCT
ecletica-204	88	5	,	,	PUNCT
ecletica-204	88	6	são	são	PROPN
ecletica-204	88	7	paulo	paulo	PROPN
ecletica-204	88	8	,	,	PUNCT
ecletica-204	88	9	35	35	NUM
ecletica-204	88	10	3	3	NUM
ecletica-204	88	11	:	:	PUNCT
ecletica-204	88	12	45	45	NUM
ecletica-204	88	13	53	53	NUM
ecletica-204	88	14	,	,	PUNCT
ecletica-204	88	15	201050	201050	NUM
ecletica-204	89	1	ecl	ecl	PROPN
ecletica-204	89	2	.	.	PROPN
ecletica-204	89	3	quím	quím	PROPN
ecletica-204	89	4	.	.	PUNCT
ecletica-204	89	5	,	,	PUNCT
ecletica-204	89	6	são	são	PROPN
ecletica-204	89	7	paulo	paulo	PROPN
ecletica-204	89	8	,	,	PUNCT
ecletica-204	89	9	35	35	NUM
ecletica-204	89	10	3	3	NUM
ecletica-204	89	11	:	:	PUNCT
ecletica-204	89	12	45	45	NUM
ecletica-204	89	13	53	53	NUM
ecletica-204	89	14	,	,	PUNCT
ecletica-204	89	15	2010	2010	NUM
ecletica-204	89	16	51	51	NUM
ecletica-204	89	17	artigo	artigo	NOUN
ecletica-204	89	18	article	article	NOUN
ecletica-204	89	19	artigo	artigo	PROPN
ecletica-204	89	20	article	article	PROPN
ecletica-204	89	21	fig	fig	NOUN
ecletica-204	89	22	4	4	NUM
ecletica-204	89	23	.	.	PUNCT
ecletica-204	90	1	linearity	linearity	NOUN
ecletica-204	90	2	of	of	ADP
ecletica-204	90	3	absorbance	absorbance	NOUN
ecletica-204	90	4	to	to	ADP
ecletica-204	90	5	concentration	concentration	NOUN
ecletica-204	90	6	of	of	ADP
ecletica-204	90	7	hantzch	hantzch	ADJ
ecletica-204	90	8	product	product	NOUN
ecletica-204	90	9	0	0	NUM
ecletica-204	90	10	0.1	0.1	NUM
ecletica-204	90	11	0.2	0.2	NUM
ecletica-204	90	12	0.3	0.3	NUM
ecletica-204	90	13	0.4	0.4	NUM
ecletica-204	90	14	0.5	0.5	NUM
ecletica-204	90	15	0.6	0.6	NUM
ecletica-204	90	16	0	0	NUM
ecletica-204	90	17	5	5	NUM
ecletica-204	90	18	10	10	NUM
ecletica-204	90	19	15	15	NUM
ecletica-204	90	20	20	20	NUM
ecletica-204	90	21	25	25	NUM
ecletica-204	90	22	30	30	NUM
ecletica-204	90	23	concentration	concentration	NOUN
ecletica-204	90	24	(	(	PUNCT
ecletica-204	90	25	μg	μg	NOUN
ecletica-204	90	26	/	/	SYM
ecletica-204	90	27	ml	ml	PROPN
ecletica-204	90	28	)	)	PUNCT
ecletica-204	90	29	ab	ab	PROPN
ecletica-204	90	30	so	so	ADV
ecletica-204	90	31	rb	rb	PROPN
ecletica-204	90	32	an	an	DET
ecletica-204	90	33	ce	ce	PROPN
ecletica-204	90	34	a	a	PRON
ecletica-204	90	35	t	t	PROPN
ecletica-204	90	36	4	4	NUM
ecletica-204	90	37	30	30	NUM
ecletica-204	90	38	nm	nm	PRON
ecletica-204	90	39	table	table	NOUN
ecletica-204	90	40	2	2	NUM
ecletica-204	90	41	.	.	X
ecletica-204	90	42	optical	optical	ADJ
ecletica-204	90	43	and	and	CCONJ
ecletica-204	90	44	regression	regression	NOUN
ecletica-204	90	45	characteristics	characteristic	NOUN
ecletica-204	90	46	,	,	PUNCT
ecletica-204	90	47	precision	precision	NOUN
ecletica-204	90	48	and	and	CCONJ
ecletica-204	90	49	accuracy	accuracy	NOUN
ecletica-204	90	50	of	of	ADP
ecletica-204	90	51	the	the	DET
ecletica-204	90	52	proposed	propose	VERB
ecletica-204	90	53	method	method	NOUN
ecletica-204	90	54	parameters	parameter	NOUN
ecletica-204	90	55	method	method	VERB
ecletica-204	90	56	b	b	PROPN
ecletica-204	90	57	λ	λ	X
ecletica-204	90	58	max	max	PROPN
ecletica-204	90	59	(	(	PUNCT
ecletica-204	90	60	nm	nm	NOUN
ecletica-204	90	61	)	)	PUNCT
ecletica-204	90	62	430	430	NUM
ecletica-204	90	63	beer	beer	NOUN
ecletica-204	90	64	’s	’s	PART
ecletica-204	90	65	law	law	NOUN
ecletica-204	90	66	limit	limit	NOUN
ecletica-204	90	67	(	(	PUNCT
ecletica-204	90	68	μg/	μg/	NOUN
ecletica-204	90	69	ml	ml	VERB
ecletica-204	90	70	)	)	PUNCT
ecletica-204	90	71	5	5	NUM
ecletica-204	90	72	25	25	NUM
ecletica-204	90	73	sandell	sandell	NOUN
ecletica-204	90	74	’s	’s	PART
ecletica-204	90	75	sensitivity	sensitivity	NOUN
ecletica-204	90	76	(	(	PUNCT
ecletica-204	90	77	μg	μg	PROPN
ecletica-204	90	78	/	/	SYM
ecletica-204	90	79	cm2/0.001	cm2/0.001	VERB
ecletica-204	90	80	abs	ab	NOUN
ecletica-204	90	81	.	.	PUNCT
ecletica-204	91	1	unit	unit	NOUN
ecletica-204	91	2	)	)	PUNCT
ecletica-204	92	1	0.0471	0.0471	NUM
ecletica-204	92	2	molar	molar	ADJ
ecletica-204	92	3	absorptivity(litre.mole-1.cm-1	absorptivity(litre.mole-1.cm-1	NOUN
ecletica-204	92	4	)	)	PUNCT
ecletica-204	92	5	1.067	1.067	NUM
ecletica-204	92	6	x	x	SYM
ecletica-204	92	7	104	104	NUM
ecletica-204	92	8	stability	stability	NOUN
ecletica-204	92	9	of	of	ADP
ecletica-204	92	10	color	color	NOUN
ecletica-204	92	11	(	(	PUNCT
ecletica-204	92	12	hours	hour	NOUN
ecletica-204	92	13	)	)	PUNCT
ecletica-204	92	14	1	1	NUM
ecletica-204	92	15	regression	regression	NOUN
ecletica-204	92	16	equation	equation	NOUN
ecletica-204	92	17	(	(	PUNCT
ecletica-204	92	18	y	y	NOUN
ecletica-204	92	19	)	)	PUNCT
ecletica-204	92	20	*	*	PUNCT
ecletica-204	93	1	intercept	intercept	NOUN
ecletica-204	93	2	(	(	PUNCT
ecletica-204	93	3	c	c	NOUN
ecletica-204	93	4	)	)	PUNCT
ecletica-204	93	5	0.0106	0.0106	NUM
ecletica-204	93	6	slope(b	slope(b	PROPN
ecletica-204	93	7	)	)	PUNCT
ecletica-204	93	8	0.0020	0.0020	NUM
ecletica-204	93	9	correlation	correlation	NOUN
ecletica-204	93	10	coeffi	coeffi	NOUN
ecletica-204	93	11	cient	cient	VERB
ecletica-204	93	12	0.9998	0.9998	NUM
ecletica-204	93	13	%	%	NOUN
ecletica-204	93	14	relative	relative	ADJ
ecletica-204	93	15	standard	standard	ADJ
ecletica-204	93	16	deviation	deviation	NOUN
ecletica-204	93	17	*	*	PUNCT
ecletica-204	93	18	*	*	PUNCT
ecletica-204	93	19	1.13	1.13	NUM
ecletica-204	93	20	%	%	NOUN
ecletica-204	93	21	range	range	NOUN
ecletica-204	93	22	of	of	ADP
ecletica-204	93	23	errors	error	NOUN
ecletica-204	93	24	0.05	0.05	NUM
ecletica-204	93	25	%	%	NOUN
ecletica-204	93	26	level	level	NOUN
ecletica-204	93	27	0.951	0.951	NUM
ecletica-204	93	28	0.01	0.01	NUM
ecletica-204	93	29	%	%	NOUN
ecletica-204	93	30	level	level	NOUN
ecletica-204	93	31	1.397	1.397	NUM
ecletica-204	93	32	limit	limit	NOUN
ecletica-204	93	33	of	of	ADP
ecletica-204	93	34	detection	detection	NOUN
ecletica-204	93	35	(	(	PUNCT
ecletica-204	93	36	μg/	μg/	NOUN
ecletica-204	93	37	ml	ml	VERB
ecletica-204	93	38	)	)	PUNCT
ecletica-204	93	39	1.947	1.947	NUM
ecletica-204	93	40	limit	limit	NOUN
ecletica-204	93	41	of	of	ADP
ecletica-204	93	42	quantifi	quantifi	ADJ
ecletica-204	93	43	cation	cation	NOUN
ecletica-204	93	44	(	(	PUNCT
ecletica-204	93	45	μg/	μg/	NOUN
ecletica-204	93	46	ml	ml	VERB
ecletica-204	93	47	)	)	PUNCT
ecletica-204	93	48	5.90	5.90	NUM
ecletica-204	93	49	*	*	PUNCT
ecletica-204	94	1	y=	y=	NUM
ecletica-204	94	2	c	c	NOUN
ecletica-204	95	1	+	+	CCONJ
ecletica-204	95	2	bx	bx	PROPN
ecletica-204	95	3	,	,	PUNCT
ecletica-204	95	4	where	where	SCONJ
ecletica-204	95	5	y	y	PROPN
ecletica-204	95	6	is	be	AUX
ecletica-204	95	7	the	the	DET
ecletica-204	95	8	absorbance	absorbance	NOUN
ecletica-204	95	9	and	and	CCONJ
ecletica-204	95	10	x	x	NOUN
ecletica-204	95	11	is	be	AUX
ecletica-204	95	12	the	the	DET
ecletica-204	95	13	concentration	concentration	NOUN
ecletica-204	95	14	of	of	ADP
ecletica-204	95	15	sitagliptin	sitagliptin	NOUN
ecletica-204	95	16	phosphate	phosphate	NOUN
ecletica-204	95	17	in	in	ADP
ecletica-204	95	18	μg	μg	PROPN
ecletica-204	95	19	/	/	SYM
ecletica-204	95	20	ml	ml	NOUN
ecletica-204	95	21	*	*	NOUN
ecletica-204	95	22	*	*	NOUN
ecletica-204	95	23	average	average	NOUN
ecletica-204	95	24	of	of	ADP
ecletica-204	95	25	six	six	NUM
ecletica-204	95	26	determinants	determinant	NOUN
ecletica-204	95	27	accuracy	accuracy	NOUN
ecletica-204	95	28	precision	precision	NOUN
ecletica-204	95	29	and	and	CCONJ
ecletica-204	95	30	recovery	recovery	NOUN
ecletica-204	95	31	studies	study	NOUN
ecletica-204	95	32	:	:	PUNCT
ecletica-204	95	33	the	the	DET
ecletica-204	95	34	accuracy	accuracy	NOUN
ecletica-204	95	35	and	and	CCONJ
ecletica-204	95	36	precision	precision	NOUN
ecletica-204	95	37	of	of	ADP
ecletica-204	95	38	the	the	DET
ecletica-204	95	39	proposed	propose	VERB
ecletica-204	95	40	method	method	NOUN
ecletica-204	95	41	was	be	AUX
ecletica-204	95	42	evaluated	evaluate	VERB
ecletica-204	95	43	by	by	ADP
ecletica-204	95	44	performing	perform	VERB
ecletica-204	95	45	fi	fi	NOUN
ecletica-204	95	46	ve	ve	AUX
ecletica-204	95	47	replicate	replicate	VERB
ecletica-204	95	48	determinations	determination	NOUN
ecletica-204	95	49	of	of	ADP
ecletica-204	95	50	stp	stp	ADJ
ecletica-204	95	51	in	in	ADP
ecletica-204	95	52	pure	pure	ADJ
ecletica-204	95	53	form	form	NOUN
ecletica-204	95	54	at	at	ADP
ecletica-204	95	55	three	three	NUM
ecletica-204	95	56	different	different	ADJ
ecletica-204	95	57	concentrations	concentration	NOUN
ecletica-204	95	58	(	(	PUNCT
ecletica-204	95	59	5	5	NUM
ecletica-204	95	60	,	,	PUNCT
ecletica-204	95	61	10	10	NUM
ecletica-204	95	62	and	and	CCONJ
ecletica-204	95	63	15	15	NUM
ecletica-204	95	64	μg	μg	NOUN
ecletica-204	95	65	/	/	SYM
ecletica-204	95	66	ml	ml	NOUN
ecletica-204	95	67	)	)	PUNCT
ecletica-204	95	68	by	by	ADP
ecletica-204	95	69	short	short	ADJ
ecletica-204	95	70	term	term	NOUN
ecletica-204	95	71	(	(	PUNCT
ecletica-204	95	72	intra	intra	ADJ
ecletica-204	95	73	day	day	NOUN
ecletica-204	95	74	)	)	PUNCT
ecletica-204	95	75	and	and	CCONJ
ecletica-204	95	76	daily	daily	ADV
ecletica-204	95	77	(	(	PUNCT
ecletica-204	95	78	inter	inter	ADJ
ecletica-204	95	79	day	day	NOUN
ecletica-204	95	80	)	)	PUNCT
ecletica-204	95	81	precisions	precision	NOUN
ecletica-204	95	82	(	(	PUNCT
ecletica-204	95	83	table	table	NOUN
ecletica-204	95	84	3	3	NUM
ecletica-204	95	85	)	)	PUNCT
ecletica-204	95	86	.	.	PUNCT
ecletica-204	96	1	the	the	DET
ecletica-204	96	2	standard	standard	ADJ
ecletica-204	96	3	analytical	analytical	ADJ
ecletica-204	96	4	errors	error	NOUN
ecletica-204	96	5	,	,	PUNCT
ecletica-204	96	6	relative	relative	ADJ
ecletica-204	96	7	standard	standard	ADJ
ecletica-204	96	8	deviations	deviation	NOUN
ecletica-204	96	9	(	(	PUNCT
ecletica-204	96	10	rsd	rsd	NOUN
ecletica-204	96	11	)	)	PUNCT
ecletica-204	96	12	and	and	CCONJ
ecletica-204	96	13	recoveries	recovery	NOUN
ecletica-204	96	14	obtained	obtain	VERB
ecletica-204	96	15	in	in	ADP
ecletica-204	96	16	the	the	DET
ecletica-204	96	17	intra	intra	ADJ
ecletica-204	96	18	day	day	NOUN
ecletica-204	96	19	and	and	CCONJ
ecletica-204	96	20	inter	inter	ADJ
ecletica-204	96	21	day	day	NOUN
ecletica-204	96	22	analysis	analysis	NOUN
ecletica-204	96	23	for	for	ADP
ecletica-204	96	24	the	the	DET
ecletica-204	96	25	proposed	propose	VERB
ecletica-204	96	26	method	method	NOUN
ecletica-204	96	27	was	be	AUX
ecletica-204	96	28	found	find	VERB
ecletica-204	96	29	to	to	PART
ecletica-204	96	30	be	be	AUX
ecletica-204	96	31	acceptable	acceptable	ADJ
ecletica-204	96	32	.	.	PUNCT
ecletica-204	97	1	thus	thus	ADV
ecletica-204	97	2	the	the	DET
ecletica-204	97	3	proposed	propose	VERB
ecletica-204	97	4	method	method	NOUN
ecletica-204	97	5	is	be	AUX
ecletica-204	97	6	effective	effective	ADJ
ecletica-204	97	7	for	for	ADP
ecletica-204	97	8	the	the	DET
ecletica-204	97	9	determination	determination	NOUN
ecletica-204	97	10	of	of	ADP
ecletica-204	97	11	stp	stp	PROPN
ecletica-204	97	12	.	.	PROPN
ecletica-204	97	13	table	table	NOUN
ecletica-204	97	14	3	3	NUM
ecletica-204	97	15	.	.	PUNCT
ecletica-204	97	16	evaluation	evaluation	NOUN
ecletica-204	97	17	of	of	ADP
ecletica-204	97	18	the	the	DET
ecletica-204	97	19	accuracy	accuracy	NOUN
ecletica-204	97	20	and	and	CCONJ
ecletica-204	97	21	precision	precision	NOUN
ecletica-204	97	22	of	of	ADP
ecletica-204	97	23	the	the	DET
ecletica-204	97	24	proposed	propose	VERB
ecletica-204	97	25	method	method	NOUN
ecletica-204	97	26	by	by	ADP
ecletica-204	97	27	intra	intra	ADJ
ecletica-204	97	28	day	day	NOUN
ecletica-204	97	29	and	and	CCONJ
ecletica-204	97	30	inter	inter	ADJ
ecletica-204	97	31	day	day	NOUN
ecletica-204	97	32	assay	assay	VERB
ecletica-204	97	33	concentration	concentration	NOUN
ecletica-204	97	34	of	of	ADP
ecletica-204	97	35	sitagliptin	sitagliptin	NOUN
ecletica-204	97	36	phosphate(μg	phosphate(μg	PROPN
ecletica-204	97	37	/	/	SYM
ecletica-204	97	38	ml	ml	NOUN
ecletica-204	97	39	)	)	PUNCT
ecletica-204	97	40	observed	observe	VERB
ecletica-204	97	41	concentration	concentration	NOUN
ecletica-204	97	42	of	of	ADP
ecletica-204	97	43	stp	stp	PROPN
ecletica-204	97	44	(	(	PUNCT
ecletica-204	97	45	μg	μg	PROPN
ecletica-204	97	46	/	/	SYM
ecletica-204	97	47	ml	ml	NOUN
ecletica-204	97	48	)	)	PUNCT
ecletica-204	97	49	intra	intra	ADJ
ecletica-204	97	50	-	-	ADJ
ecletica-204	97	51	day	day	ADJ
ecletica-204	97	52	inter	inter	ADJ
ecletica-204	97	53	-	-	NOUN
ecletica-204	97	54	day	day	ADJ
ecletica-204	97	55	mean	mean	NOUN
ecletica-204	97	56	*	*	NOUN
ecletica-204	97	57	error	error	NOUN
ecletica-204	97	58	(	(	PUNCT
ecletica-204	97	59	%	%	INTJ
ecletica-204	97	60	)	)	PUNCT
ecletica-204	97	61	rsd	rsd	NOUN
ecletica-204	97	62	(	(	PUNCT
ecletica-204	97	63	%	%	NOUN
ecletica-204	97	64	)	)	PUNCT
ecletica-204	97	65	recovery	recovery	NOUN
ecletica-204	97	66	(	(	PUNCT
ecletica-204	97	67	%	%	INTJ
ecletica-204	97	68	)	)	PUNCT
ecletica-204	97	69	mean	mean	NOUN
ecletica-204	97	70	*	*	PUNCT
ecletica-204	97	71	error	error	NOUN
ecletica-204	97	72	(	(	PUNCT
ecletica-204	97	73	%	%	INTJ
ecletica-204	97	74	)	)	PUNCT
ecletica-204	97	75	rsd	rsd	NOUN
ecletica-204	97	76	(	(	PUNCT
ecletica-204	97	77	%	%	NOUN
ecletica-204	97	78	)	)	PUNCT
ecletica-204	97	79	recovery	recovery	NOUN
ecletica-204	97	80	(	(	PUNCT
ecletica-204	97	81	%	%	NOUN
ecletica-204	97	82	)	)	PUNCT
ecletica-204	97	83	5	5	NUM
ecletica-204	97	84	4.97	4.97	NUM
ecletica-204	97	85	0.60	0.60	NUM
ecletica-204	97	86	0.56	0.56	NUM
ecletica-204	97	87	99.40	99.40	NUM
ecletica-204	97	88	5.02	5.02	NUM
ecletica-204	97	89	0.40	0.40	NUM
ecletica-204	97	90	0.48	0.48	NUM
ecletica-204	97	91	100.4	100.4	NUM
ecletica-204	97	92	10	10	NUM
ecletica-204	97	93	10.10	10.10	NUM
ecletica-204	97	94	1.00	1.00	NUM
ecletica-204	97	95	0.39	0.39	NUM
ecletica-204	97	96	101.00	101.00	NUM
ecletica-204	97	97	9.98	9.98	NUM
ecletica-204	97	98	0.20	0.20	NUM
ecletica-204	97	99	0.19	0.19	NUM
ecletica-204	97	100	99.80	99.80	NUM
ecletica-204	97	101	15	15	NUM
ecletica-204	97	102	15.06	15.06	NUM
ecletica-204	97	103	0.40	0.40	NUM
ecletica-204	97	104	0.43	0.43	NUM
ecletica-204	97	105	100.40	100.40	NUM
ecletica-204	97	106	14.97	14.97	NUM
ecletica-204	97	107	0.20	0.20	NUM
ecletica-204	97	108	0.73	0.73	NUM
ecletica-204	97	109	99.80	99.80	NUM
ecletica-204	97	110	*	*	PUNCT
ecletica-204	97	111	for	for	ADP
ecletica-204	97	112	fi	fi	NOUN
ecletica-204	97	113	ve	ve	NOUN
ecletica-204	97	114	determinants	determinant	VERB
ecletica-204	97	115	the	the	DET
ecletica-204	97	116	accuracy	accuracy	NOUN
ecletica-204	97	117	of	of	ADP
ecletica-204	97	118	the	the	DET
ecletica-204	97	119	proposed	propose	VERB
ecletica-204	97	120	method	method	NOUN
ecletica-204	97	121	was	be	AUX
ecletica-204	97	122	further	far	ADV
ecletica-204	97	123	checked	check	VERB
ecletica-204	97	124	by	by	ADP
ecletica-204	97	125	performing	perform	VERB
ecletica-204	97	126	recovery	recovery	NOUN
ecletica-204	97	127	experiments	experiment	NOUN
ecletica-204	97	128	through	through	ADP
ecletica-204	97	129	standard	standard	ADJ
ecletica-204	97	130	addition	addition	NOUN
ecletica-204	97	131	technique	technique	NOUN
ecletica-204	97	132	.	.	PUNCT
ecletica-204	98	1	for	for	ADP
ecletica-204	98	2	this	this	DET
ecletica-204	98	3	purpose	purpose	NOUN
ecletica-204	98	4	,	,	PUNCT
ecletica-204	98	5	a	a	DET
ecletica-204	98	6	known	know	VERB
ecletica-204	98	7	amount	amount	NOUN
ecletica-204	98	8	of	of	ADP
ecletica-204	98	9	pure	pure	ADJ
ecletica-204	98	10	stp	stp	PROPN
ecletica-204	98	11	was	be	AUX
ecletica-204	98	12	added	add	VERB
ecletica-204	98	13	to	to	ADP
ecletica-204	98	14	pre	pre	VERB
ecletica-204	98	15	-	-	ADJ
ecletica-204	98	16	analyzed	analyze	VERB
ecletica-204	98	17	dosage	dosage	NOUN
ecletica-204	98	18	forms	form	NOUN
ecletica-204	98	19	and	and	CCONJ
ecletica-204	98	20	then	then	ADV
ecletica-204	98	21	determined	determine	VERB
ecletica-204	98	22	by	by	ADP
ecletica-204	98	23	the	the	DET
ecletica-204	98	24	recommended	recommend	VERB
ecletica-204	98	25	procedure	procedure	NOUN
ecletica-204	98	26	.	.	PUNCT
ecletica-204	99	1	the	the	DET
ecletica-204	99	2	results	result	NOUN
ecletica-204	99	3	(	(	PUNCT
ecletica-204	99	4	table	table	NOUN
ecletica-204	99	5	4	4	NUM
ecletica-204	99	6	)	)	PUNCT
ecletica-204	99	7	shown	show	VERB
ecletica-204	99	8	that	that	SCONJ
ecletica-204	99	9	the	the	DET
ecletica-204	99	10	mean	mean	ADJ
ecletica-204	99	11	recovery	recovery	NOUN
ecletica-204	99	12	and	and	CCONJ
ecletica-204	99	13	relative	relative	ADJ
ecletica-204	99	14	standard	standard	ADJ
ecletica-204	99	15	deviation	deviation	NOUN
ecletica-204	99	16	(	(	PUNCT
ecletica-204	99	17	rsd	rsd	NOUN
ecletica-204	99	18	)	)	PUNCT
ecletica-204	99	19	were	be	AUX
ecletica-204	99	20	in	in	ADP
ecletica-204	99	21	the	the	DET
ecletica-204	99	22	range	range	NOUN
ecletica-204	99	23	of	of	ADP
ecletica-204	99	24	99.94–100.12	99.94–100.12	NUM
ecletica-204	99	25	and	and	CCONJ
ecletica-204	99	26	0.26–0.54	0.26–0.54	NUM
ecletica-204	99	27	%	%	NOUN
ecletica-204	99	28	indicating	indicate	VERB
ecletica-204	99	29	the	the	DET
ecletica-204	99	30	reproducibility	reproducibility	NOUN
ecletica-204	99	31	of	of	ADP
ecletica-204	99	32	the	the	DET
ecletica-204	99	33	method	method	NOUN
ecletica-204	99	34	.	.	PUNCT
ecletica-204	100	1	no	no	DET
ecletica-204	100	2	interference	interference	NOUN
ecletica-204	100	3	from	from	ADP
ecletica-204	100	4	the	the	DET
ecletica-204	100	5	common	common	ADJ
ecletica-204	100	6	excipients	excipient	NOUN
ecletica-204	100	7	was	be	AUX
ecletica-204	100	8	observed	observe	VERB
ecletica-204	100	9	.	.	PUNCT
ecletica-204	101	1	table	table	NOUN
ecletica-204	101	2	4	4	NUM
ecletica-204	101	3	.	.	PUNCT
ecletica-204	102	1	determination	determination	NOUN
ecletica-204	102	2	of	of	ADP
ecletica-204	102	3	stp	stp	PROPN
ecletica-204	102	4	in	in	ADP
ecletica-204	102	5	pharmaceutical	pharmaceutical	NOUN
ecletica-204	102	6	formulations	formulation	NOUN
ecletica-204	102	7	by	by	ADP
ecletica-204	102	8	standard	standard	ADJ
ecletica-204	102	9	addition	addition	NOUN
ecletica-204	102	10	technique	technique	NOUN
ecletica-204	102	11	amount	amount	NOUN
ecletica-204	102	12	of	of	ADP
ecletica-204	102	13	drug	drug	NOUN
ecletica-204	102	14	added(μg	added(μg	NOUN
ecletica-204	102	15	)	)	PUNCT
ecletica-204	102	16	theoretical	theoretical	ADJ
ecletica-204	102	17	amount(μg	amount(μg	NOUN
ecletica-204	102	18	)	)	PUNCT
ecletica-204	102	19	mean	mean	NOUN
ecletica-204	102	20	amount	amount	NOUN
ecletica-204	102	21	(	(	PUNCT
ecletica-204	102	22	μg	μg	NOUN
ecletica-204	102	23	)	)	PUNCT
ecletica-204	102	24	recovered(n=5	recovered(n=5	NUM
ecletica-204	102	25	)	)	PUNCT
ecletica-204	102	26	mean	mean	ADJ
ecletica-204	102	27	%	%	NOUN
ecletica-204	102	28	of	of	ADP
ecletica-204	102	29	recovery(n=5	recovery(n=5	PROPN
ecletica-204	102	30	)	)	PUNCT
ecletica-204	102	31	rsd	rsd	NOUN
ecletica-204	102	32	(	(	PUNCT
ecletica-204	102	33	%	%	NOUN
ecletica-204	102	34	)	)	PUNCT
ecletica-204	103	1	50	50	NUM
ecletica-204	103	2	50	50	NUM
ecletica-204	103	3	100.12	100.12	NUM
ecletica-204	103	4	100.12	100.12	NUM
ecletica-204	103	5	0.26	0.26	NUM
ecletica-204	103	6	100	100	NUM
ecletica-204	103	7	100	100	NUM
ecletica-204	103	8	199.89	199.89	NUM
ecletica-204	103	9	99.94	99.94	NUM
ecletica-204	103	10	0.54	0.54	NUM
ecletica-204	103	11	analysis	analysis	NOUN
ecletica-204	103	12	of	of	ADP
ecletica-204	103	13	pharmaceutical	pharmaceutical	ADJ
ecletica-204	103	14	preparations	preparation	NOUN
ecletica-204	103	15	the	the	DET
ecletica-204	103	16	proposed	propose	VERB
ecletica-204	103	17	methods	method	NOUN
ecletica-204	103	18	were	be	AUX
ecletica-204	103	19	applied	apply	VERB
ecletica-204	103	20	to	to	ADP
ecletica-204	103	21	the	the	DET
ecletica-204	103	22	analysis	analysis	NOUN
ecletica-204	103	23	of	of	ADP
ecletica-204	103	24	stp	stp	PROPN
ecletica-204	103	25	in	in	ADP
ecletica-204	103	26	pharmaceutical	pharmaceutical	ADJ
ecletica-204	103	27	dosage	dosage	NOUN
ecletica-204	103	28	forms	form	NOUN
ecletica-204	103	29	and	and	CCONJ
ecletica-204	103	30	the	the	DET
ecletica-204	103	31	results	result	NOUN
ecletica-204	103	32	were	be	AUX
ecletica-204	103	33	statistically	statistically	ADV
ecletica-204	103	34	compared	compare	VERB
ecletica-204	103	35	with	with	ADP
ecletica-204	103	36	uv	uv	NOUN
ecletica-204	103	37	method	method	NOUN
ecletica-204	103	38	by	by	ADP
ecletica-204	103	39	calculating	calculate	VERB
ecletica-204	103	40	the	the	DET
ecletica-204	103	41	student	student	NOUN
ecletica-204	103	42	’s	’s	PART
ecletica-204	103	43	tand	tand	PROPN
ecletica-204	104	1	f	f	X
ecletica-204	104	2	-	-	PUNCT
ecletica-204	104	3	values	value	NOUN
ecletica-204	104	4	.	.	PUNCT
ecletica-204	105	1	the	the	DET
ecletica-204	105	2	evaluated	evaluate	VERB
ecletica-204	105	3	tand	tand	NOUN
ecletica-204	105	4	f	f	X
ecletica-204	105	5	-	-	PUNCT
ecletica-204	105	6	values	value	NOUN
ecletica-204	105	7	were	be	AUX
ecletica-204	105	8	less	less	ADJ
ecletica-204	105	9	than	than	ADP
ecletica-204	105	10	the	the	DET
ecletica-204	105	11	tabulated	tabulate	VERB
ecletica-204	105	12	values	value	NOUN
ecletica-204	105	13	at	at	ADP
ecletica-204	105	14	the	the	DET
ecletica-204	105	15	95	95	NUM
ecletica-204	105	16	%	%	NOUN
ecletica-204	105	17	confi	confi	NOUN
ecletica-204	105	18	dence	dence	NOUN
ecletica-204	105	19	level	level	NOUN
ecletica-204	105	20	for	for	ADP
ecletica-204	105	21	eight	eight	NUM
ecletica-204	105	22	degrees	degree	NOUN
ecletica-204	105	23	of	of	ADP
ecletica-204	105	24	freedom	freedom	NOUN
ecletica-204	105	25	(	(	PUNCT
ecletica-204	105	26	16	16	NUM
ecletica-204	105	27	)	)	PUNCT
ecletica-204	105	28	,	,	PUNCT
ecletica-204	105	29	as	as	SCONJ
ecletica-204	105	30	revealed	reveal	VERB
ecletica-204	105	31	by	by	ADP
ecletica-204	105	32	the	the	DET
ecletica-204	105	33	results	result	NOUN
ecletica-204	105	34	complied	comply	VERB
ecletica-204	105	35	in	in	ADP
ecletica-204	105	36	table	table	NOUN
ecletica-204	105	37	5	5	NUM
ecletica-204	105	38	.	.	PUNCT
ecletica-204	106	1	this	this	PRON
ecletica-204	106	2	actually	actually	ADV
ecletica-204	106	3	suggests	suggest	VERB
ecletica-204	106	4	that	that	SCONJ
ecletica-204	106	5	the	the	DET
ecletica-204	106	6	proposed	propose	VERB
ecletica-204	106	7	methods	method	NOUN
ecletica-204	106	8	are	be	AUX
ecletica-204	106	9	accurate	accurate	ADJ
ecletica-204	106	10	and	and	CCONJ
ecletica-204	106	11	precise	precise	ADJ
ecletica-204	106	12	as	as	ADP
ecletica-204	106	13	the	the	DET
ecletica-204	106	14	uv	uv	NOUN
ecletica-204	106	15	method	method	NOUN
ecletica-204	106	16	.	.	PUNCT
ecletica-204	107	1	ecl	ecl	PROPN
ecletica-204	107	2	.	.	PROPN
ecletica-204	107	3	quím	quím	PROPN
ecletica-204	107	4	.	.	PUNCT
ecletica-204	108	1	,	,	PUNCT
ecletica-204	108	2	são	são	PROPN
ecletica-204	108	3	paulo	paulo	PROPN
ecletica-204	108	4	,	,	PUNCT
ecletica-204	108	5	35	35	NUM
ecletica-204	108	6	3	3	NUM
ecletica-204	108	7	:	:	PUNCT
ecletica-204	108	8	45	45	NUM
ecletica-204	108	9	53	53	NUM
ecletica-204	108	10	,	,	PUNCT
ecletica-204	108	11	201052	201052	NUM
ecletica-204	109	1	ecl	ecl	PROPN
ecletica-204	109	2	.	.	PROPN
ecletica-204	109	3	quím	quím	PROPN
ecletica-204	109	4	.	.	PUNCT
ecletica-204	109	5	,	,	PUNCT
ecletica-204	109	6	são	são	PROPN
ecletica-204	109	7	paulo	paulo	PROPN
ecletica-204	109	8	,	,	PUNCT
ecletica-204	109	9	35	35	NUM
ecletica-204	109	10	3	3	NUM
ecletica-204	109	11	:	:	PUNCT
ecletica-204	109	12	45	45	NUM
ecletica-204	109	13	53	53	NUM
ecletica-204	109	14	,	,	PUNCT
ecletica-204	109	15	2010	2010	NUM
ecletica-204	109	16	53	53	NUM
ecletica-204	109	17	artigo	artigo	PROPN
ecletica-204	109	18	article	article	NOUN
ecletica-204	109	19	artigo	artigo	PROPN
ecletica-204	109	20	article	article	NOUN
ecletica-204	109	21	table	table	VERB
ecletica-204	109	22	5	5	NUM
ecletica-204	109	23	.	.	PUNCT
ecletica-204	109	24	results	result	NOUN
ecletica-204	109	25	of	of	ADP
ecletica-204	109	26	analysis	analysis	NOUN
ecletica-204	109	27	of	of	ADP
ecletica-204	109	28	tablet	tablet	NOUN
ecletica-204	109	29	formulations	formulation	NOUN
ecletica-204	109	30	containing	contain	VERB
ecletica-204	109	31	stp	stp	PROPN
ecletica-204	109	32	formulations	formulation	NOUN
ecletica-204	109	33	labeled	label	VERB
ecletica-204	109	34	amount(mg	amount(mg	NOUN
ecletica-204	109	35	)	)	PUNCT
ecletica-204	109	36	%	%	NOUN
ecletica-204	109	37	found	find	VERB
ecletica-204	109	38	*	*	PROPN
ecletica-204	109	39	*	*	PROPN
ecletica-204	109	40	±	±	NUM
ecletica-204	109	41	s.d	s.d	PROPN
ecletica-204	109	42	reference	reference	NOUN
ecletica-204	109	43	method	method	NOUN
ecletica-204	109	44	*	*	ADP
ecletica-204	109	45	proposed	propose	VERB
ecletica-204	109	46	method	method	NOUN
ecletica-204	109	47	t	t	PROPN
ecletica-204	109	48	-	-	PUNCT
ecletica-204	109	49	test	test	NOUN
ecletica-204	109	50	f	f	NOUN
ecletica-204	109	51	-	-	PUNCT
ecletica-204	109	52	test	test	NOUN
ecletica-204	109	53	tablet	tablet	NOUN
ecletica-204	109	54	i	i	PRON
ecletica-204	109	55	100	100	NUM
ecletica-204	109	56	99.83	99.83	NUM
ecletica-204	109	57	±	±	NUM
ecletica-204	109	58	0.24	0.24	NUM
ecletica-204	109	59	99.94	99.94	NUM
ecletica-204	109	60	2.01	2.01	NUM
ecletica-204	109	61	5.01	5.01	NUM
ecletica-204	109	62	tablet	tablet	NOUN
ecletica-204	109	63	ii	ii	PROPN
ecletica-204	109	64	50	50	NUM
ecletica-204	109	65	100.16	100.16	NUM
ecletica-204	109	66	±	±	NOUN
ecletica-204	109	67	0.56	0.56	NUM
ecletica-204	109	68	98.82	98.82	NUM
ecletica-204	109	69	1.58	1.58	NUM
ecletica-204	109	70	4.25	4.25	NUM
ecletica-204	109	71	tablet	tablet	NOUN
ecletica-204	109	72	iii	iii	NUM
ecletica-204	110	1	25	25	NUM
ecletica-204	110	2	99.83±0.24	99.83±0.24	NUM
ecletica-204	110	3	99.93	99.93	NUM
ecletica-204	110	4	1.56	1.56	NUM
ecletica-204	110	5	3.45	3.45	NUM
ecletica-204	110	6	*	*	PUNCT
ecletica-204	110	7	*	*	PUNCT
ecletica-204	110	8	recovery	recovery	NOUN
ecletica-204	110	9	amount	amount	NOUN
ecletica-204	110	10	was	be	AUX
ecletica-204	110	11	the	the	DET
ecletica-204	110	12	average	average	NOUN
ecletica-204	110	13	of	of	ADP
ecletica-204	110	14	fi	fi	NOUN
ecletica-204	110	15	ve	ve	NOUN
ecletica-204	110	16	determinants	determinant	NOUN
ecletica-204	110	17	*	*	PUNCT
ecletica-204	110	18	uv	uv	NOUN
ecletica-204	110	19	method	method	NOUN
ecletica-204	110	20	developed	develop	VERB
ecletica-204	110	21	in	in	ADP
ecletica-204	110	22	the	the	DET
ecletica-204	110	23	laboratory	laboratory	NOUN
ecletica-204	110	24	tabulated	tabulate	VERB
ecletica-204	110	25	t	t	NOUN
ecletica-204	110	26	-	-	PUNCT
ecletica-204	110	27	value	value	NOUN
ecletica-204	110	28	at	at	ADP
ecletica-204	110	29	95	95	NUM
ecletica-204	110	30	%	%	NOUN
ecletica-204	110	31	confi	confi	NOUN
ecletica-204	110	32	dence	dence	NOUN
ecletica-204	110	33	level	level	NOUN
ecletica-204	110	34	is	be	AUX
ecletica-204	110	35	2.306	2.306	NUM
ecletica-204	110	36	tabulated	tabulate	VERB
ecletica-204	110	37	f	f	NOUN
ecletica-204	110	38	-	-	PUNCT
ecletica-204	110	39	value	value	NOUN
ecletica-204	110	40	at	at	ADP
ecletica-204	110	41	95	95	NUM
ecletica-204	110	42	%	%	NOUN
ecletica-204	110	43	confi	confi	NOUN
ecletica-204	110	44	dence	dence	NOUN
ecletica-204	110	45	level	level	NOUN
ecletica-204	110	46	is	be	AUX
ecletica-204	110	47	6.39	6.39	NUM
ecletica-204	110	48	conclusions	conclusion	NOUN
ecletica-204	110	49	the	the	DET
ecletica-204	110	50	proposed	propose	VERB
ecletica-204	110	51	method	method	NOUN
ecletica-204	110	52	was	be	AUX
ecletica-204	110	53	quite	quite	ADV
ecletica-204	110	54	simple	simple	ADJ
ecletica-204	110	55	and	and	CCONJ
ecletica-204	110	56	do	do	AUX
ecletica-204	110	57	not	not	PART
ecletica-204	110	58	require	require	VERB
ecletica-204	110	59	any	any	DET
ecletica-204	110	60	pretreatment	pretreatment	NOUN
ecletica-204	110	61	of	of	ADP
ecletica-204	110	62	the	the	DET
ecletica-204	110	63	drug	drug	NOUN
ecletica-204	110	64	and	and	CCONJ
ecletica-204	110	65	tedious	tedious	ADJ
ecletica-204	110	66	extraction	extraction	NOUN
ecletica-204	110	67	procedure	procedure	NOUN
ecletica-204	110	68	.	.	PUNCT
ecletica-204	111	1	the	the	DET
ecletica-204	111	2	methods	method	NOUN
ecletica-204	111	3	have	have	VERB
ecletica-204	111	4	wider	wide	ADJ
ecletica-204	111	5	linear	linear	ADJ
ecletica-204	111	6	range	range	NOUN
ecletica-204	111	7	with	with	ADP
ecletica-204	111	8	good	good	ADJ
ecletica-204	111	9	accuracy	accuracy	NOUN
ecletica-204	111	10	and	and	CCONJ
ecletica-204	111	11	precision	precision	NOUN
ecletica-204	111	12	.	.	PUNCT
ecletica-204	112	1	hence	hence	ADV
ecletica-204	112	2	,	,	PUNCT
ecletica-204	112	3	the	the	DET
ecletica-204	112	4	data	datum	NOUN
ecletica-204	112	5	presented	present	VERB
ecletica-204	112	6	in	in	ADP
ecletica-204	112	7	the	the	DET
ecletica-204	112	8	manuscript	manuscript	NOUN
ecletica-204	112	9	“	"	PUNCT
ecletica-204	112	10	development	development	NOUN
ecletica-204	112	11	and	and	CCONJ
ecletica-204	112	12	validation	validation	NOUN
ecletica-204	112	13	of	of	ADP
ecletica-204	112	14	a	a	DET
ecletica-204	112	15	spectrophotometric	spectrophotometric	ADJ
ecletica-204	112	16	method	method	NOUN
ecletica-204	112	17	for	for	ADP
ecletica-204	112	18	the	the	DET
ecletica-204	112	19	determination	determination	NOUN
ecletica-204	112	20	of	of	ADP
ecletica-204	112	21	a	a	DET
ecletica-204	112	22	dpp-4	dpp-4	ADJ
ecletica-204	112	23	inhibitor	inhibitor	NOUN
ecletica-204	112	24	,	,	PUNCT
ecletica-204	112	25	sitagliptin	sitagliptin	NOUN
ecletica-204	112	26	,	,	PUNCT
ecletica-204	112	27	in	in	ADP
ecletica-204	112	28	its	its	PRON
ecletica-204	112	29	pharmaceutical	pharmaceutical	ADJ
ecletica-204	112	30	preparations	preparation	NOUN
ecletica-204	112	31	”	"	PUNCT
ecletica-204	112	32	demonstrate	demonstrate	VERB
ecletica-204	112	33	that	that	SCONJ
ecletica-204	112	34	the	the	DET
ecletica-204	112	35	proposed	propose	VERB
ecletica-204	112	36	method	method	NOUN
ecletica-204	112	37	was	be	AUX
ecletica-204	112	38	accurate	accurate	ADJ
ecletica-204	112	39	,	,	PUNCT
ecletica-204	112	40	precise	precise	ADJ
ecletica-204	112	41	,	,	PUNCT
ecletica-204	112	42	linear	linear	ADJ
ecletica-204	112	43	,	,	PUNCT
ecletica-204	112	44	selective	selective	ADJ
ecletica-204	112	45	and	and	CCONJ
ecletica-204	112	46	offer	offer	VERB
ecletica-204	112	47	advantages	advantage	NOUN
ecletica-204	112	48	of	of	ADP
ecletica-204	112	49	reagent	reagent	ADJ
ecletica-204	112	50	availability	availability	NOUN
ecletica-204	112	51	and	and	CCONJ
ecletica-204	112	52	stability	stability	NOUN
ecletica-204	112	53	,	,	PUNCT
ecletica-204	112	54	less	less	ADJ
ecletica-204	112	55	time	time	NOUN
ecletica-204	112	56	consumption	consumption	NOUN
ecletica-204	112	57	and	and	CCONJ
ecletica-204	112	58	high	high	ADJ
ecletica-204	112	59	sensitivity	sensitivity	NOUN
ecletica-204	112	60	.	.	PUNCT
ecletica-204	113	1	thus	thus	ADV
ecletica-204	113	2	it	it	PRON
ecletica-204	113	3	can	can	AUX
ecletica-204	113	4	be	be	AUX
ecletica-204	113	5	extended	extend	VERB
ecletica-204	113	6	for	for	ADP
ecletica-204	113	7	routine	routine	ADJ
ecletica-204	113	8	analysis	analysis	NOUN
ecletica-204	113	9	of	of	ADP
ecletica-204	113	10	stp	stp	PROPN
ecletica-204	113	11	in	in	ADP
ecletica-204	113	12	pharmaceutical	pharmaceutical	NOUN
ecletica-204	113	13	industries	industry	NOUN
ecletica-204	113	14	,	,	PUNCT
ecletica-204	113	15	hospitals	hospital	NOUN
ecletica-204	113	16	and	and	CCONJ
ecletica-204	113	17	research	research	NOUN
ecletica-204	113	18	laboratories	laboratory	NOUN
ecletica-204	113	19	.	.	PUNCT
ecletica-204	114	1	unlike	unlike	ADP
ecletica-204	114	2	the	the	DET
ecletica-204	114	3	lc	lc	PROPN
ecletica-204	114	4	/	/	SYM
ecletica-204	114	5	ms	ms	NOUN
ecletica-204	114	6	procedure	procedure	NOUN
ecletica-204	114	7	and	and	CCONJ
ecletica-204	114	8	high	high	ADJ
ecletica-204	114	9	performance	performance	NOUN
ecletica-204	114	10	liquid	liquid	NOUN
ecletica-204	114	11	chromatography	chromatography	NOUN
ecletica-204	114	12	procedures	procedure	NOUN
ecletica-204	114	13	,	,	PUNCT
ecletica-204	114	14	the	the	DET
ecletica-204	114	15	uv	uv	NOUN
ecletica-204	114	16	-	-	PUNCT
ecletica-204	114	17	visible	visible	ADJ
ecletica-204	114	18	spectrophotometer	spectrophotometer	NOUN
ecletica-204	114	19	instrument	instrument	NOUN
ecletica-204	114	20	is	be	AUX
ecletica-204	114	21	simple	simple	ADJ
ecletica-204	114	22	and	and	CCONJ
ecletica-204	114	23	not	not	PART
ecletica-204	114	24	of	of	ADP
ecletica-204	114	25	high	high	ADJ
ecletica-204	114	26	cost	cost	NOUN
ecletica-204	114	27	,	,	PUNCT
ecletica-204	114	28	on	on	ADP
ecletica-204	114	29	the	the	DET
ecletica-204	114	30	other	other	ADJ
ecletica-204	114	31	hand	hand	NOUN
ecletica-204	114	32	in	in	ADP
ecletica-204	114	33	terms	term	NOUN
ecletica-204	114	34	of	of	ADP
ecletica-204	114	35	simplicity	simplicity	NOUN
ecletica-204	114	36	and	and	CCONJ
ecletica-204	114	37	expense	expense	NOUN
ecletica-204	114	38	,	,	PUNCT
ecletica-204	114	39	the	the	DET
ecletica-204	114	40	method	method	NOUN
ecletica-204	114	41	could	could	AUX
ecletica-204	114	42	be	be	AUX
ecletica-204	114	43	considered	consider	VERB
ecletica-204	114	44	superior	superior	ADJ
ecletica-204	114	45	in	in	ADP
ecletica-204	114	46	comparison	comparison	NOUN
ecletica-204	114	47	with	with	ADP
ecletica-204	114	48	the	the	DET
ecletica-204	114	49	previously	previously	ADV
ecletica-204	114	50	reported	report	VERB
ecletica-204	114	51	methods	method	NOUN
ecletica-204	114	52	.	.	PUNCT
ecletica-204	115	1	moreover	moreover	ADV
ecletica-204	115	2	the	the	DET
ecletica-204	115	3	methods	method	NOUN
ecletica-204	115	4	are	be	AUX
ecletica-204	115	5	free	free	ADJ
ecletica-204	115	6	from	from	ADP
ecletica-204	115	7	interferences	interference	NOUN
ecletica-204	115	8	by	by	ADP
ecletica-204	115	9	common	common	ADJ
ecletica-204	115	10	additives	additive	NOUN
ecletica-204	115	11	and	and	CCONJ
ecletica-204	115	12	excipients	excipient	NOUN
ecletica-204	115	13	.	.	PUNCT
ecletica-204	116	1	acknowledgements	acknowledgement	NOUN
ecletica-204	116	2	the	the	DET
ecletica-204	116	3	authors	author	NOUN
ecletica-204	116	4	are	be	AUX
ecletica-204	116	5	grateful	grateful	ADJ
ecletica-204	116	6	to	to	ADP
ecletica-204	116	7	the	the	DET
ecletica-204	116	8	management	management	NOUN
ecletica-204	116	9	of	of	ADP
ecletica-204	116	10	j.k.c	j.k.c	PROPN
ecletica-204	116	11	college	college	PROPN
ecletica-204	116	12	,	,	PUNCT
ecletica-204	116	13	guntur	guntur	PROPN
ecletica-204	116	14	and	and	CCONJ
ecletica-204	116	15	management	management	NOUN
ecletica-204	116	16	of	of	ADP
ecletica-204	116	17	siddhartha	siddhartha	PROPN
ecletica-204	116	18	academy	academy	PROPN
ecletica-204	116	19	,	,	PUNCT
ecletica-204	116	20	vijayawada	vijayawada	PROPN
ecletica-204	116	21	for	for	ADP
ecletica-204	116	22	their	their	PRON
ecletica-204	116	23	continuous	continuous	ADJ
ecletica-204	116	24	support	support	NOUN
ecletica-204	116	25	and	and	CCONJ
ecletica-204	116	26	encouragement	encouragement	NOUN
ecletica-204	116	27	for	for	ADP
ecletica-204	116	28	providing	provide	VERB
ecletica-204	116	29	the	the	DET
ecletica-204	116	30	necessary	necessary	ADJ
ecletica-204	116	31	facilities	facility	NOUN
ecletica-204	116	32	.	.	PUNCT
ecletica-204	117	1	references	reference	NOUN
ecletica-204	117	2	[	[	X
ecletica-204	117	3	1	1	NUM
ecletica-204	117	4	]	]	X
ecletica-204	117	5	g.	g.	PROPN
ecletica-204	117	6	herman	herman	PROPN
ecletica-204	117	7	,	,	PUNCT
ecletica-204	117	8	c.	c.	PROPN
ecletica-204	117	9	stevens	stevens	PROPN
ecletica-204	117	10	,	,	PUNCT
ecletica-204	117	11	k.	k.	PROPN
ecletica-204	117	12	van	van	PROPN
ecletica-204	117	13	dyck	dyck	PROPN
ecletica-204	117	14	,	,	PUNCT
ecletica-204	117	15	a.	a.	NOUN
ecletica-204	117	16	bergman	bergman	PROPN
ecletica-204	117	17	,	,	PUNCT
ecletica-204	117	18	yi	yi	PROPN
ecletica-204	117	19	b	b	PROPN
ecletica-204	117	20	,	,	PUNCT
ecletica-204	117	21	m.	m.	PROPN
ecletica-204	117	22	de	de	PROPN
ecletica-204	117	23	smet	smet	PROPN
ecletica-204	117	24	,	,	PUNCT
ecletica-204	117	25	k.	k.	PROPN
ecletica-204	117	26	snyder	snyder	PROPN
ecletica-204	117	27	,	,	PUNCT
ecletica-204	117	28	d.	d.	PROPN
ecletica-204	117	29	hilliard	hilliard	PROPN
ecletica-204	117	30	,	,	PUNCT
ecletica-204	117	31	m.	m.	NOUN
ecletica-204	117	32	tanen	tanen	NOUN
ecletica-204	117	33	,	,	PUNCT
ecletica-204	117	34	w.	w.	PROPN
ecletica-204	117	35	tanaka	tanaka	PROPN
ecletica-204	117	36	,	,	PUNCT
ecletica-204	117	37	a.	a.	PROPN
ecletica-204	117	38	wang	wang	PROPN
ecletica-204	117	39	,	,	PUNCT
ecletica-204	117	40	w.	w.	PROPN
ecletica-204	117	41	zeng	zeng	PROPN
ecletica-204	117	42	,	,	PUNCT
ecletica-204	117	43	d.	d.	PROPN
ecletica-204	117	44	musson	musson	PROPN
ecletica-204	117	45	,	,	PUNCT
ecletica-204	117	46	g.	g.	PROPN
ecletica-204	117	47	winchell	winchell	PROPN
ecletica-204	117	48	,	,	PUNCT
ecletica-204	117	49	m.	m.	NOUN
ecletica-204	117	50	davies	davy	NOUN
ecletica-204	117	51	,	,	PUNCT
ecletica-204	117	52	s.	s.	PROPN
ecletica-204	117	53	ramael	ramael	PROPN
ecletica-204	117	54	,	,	PUNCT
ecletica-204	117	55	k.	k.	PROPN
ecletica-204	117	56	gottesdiener	gottesdiener	PROPN
ecletica-204	117	57	and	and	CCONJ
ecletica-204	117	58	j.	j.	PROPN
ecletica-204	117	59	wagner	wagner	PROPN
ecletica-204	117	60	,	,	PUNCT
ecletica-204	117	61	clinical	clinical	ADJ
ecletica-204	117	62	pharmacology	pharmacology	NOUN
ecletica-204	117	63	and	and	CCONJ
ecletica-204	117	64	therapeutics	therapeutic	NOUN
ecletica-204	117	65	.	.	PUNCT
ecletica-204	118	1	78(6	78(6	NUM
ecletica-204	118	2	)	)	PUNCT
ecletica-204	118	3	(	(	PUNCT
ecletica-204	118	4	2005	2005	NUM
ecletica-204	118	5	)	)	PUNCT
ecletica-204	118	6	675	675	NUM
ecletica-204	118	7	.	.	PUNCT
ecletica-204	119	1	[	[	X
ecletica-204	119	2	2	2	NUM
ecletica-204	119	3	]	]	X
ecletica-204	119	4	januvia	januvia	PROPN
ecletica-204	119	5	side	side	PROPN
ecletica-204	119	6	effects	effect	NOUN
ecletica-204	119	7	&	&	CCONJ
ecletica-204	119	8	drug	drug	NOUN
ecletica-204	119	9	interactions	interaction	NOUN
ecletica-204	119	10	.	.	PUNCT
ecletica-204	120	1	rxlist	rxlist	NOUN
ecletica-204	120	2	.	.	PUNCT
ecletica-204	120	3	com	com	NOUN
ecletica-204	120	4	,	,	PUNCT
ecletica-204	120	5	2007	2007	NUM
ecletica-204	120	6	.	.	PUNCT
ecletica-204	121	1	[	[	X
ecletica-204	121	2	3	3	X
ecletica-204	121	3	]	]	X
ecletica-204	121	4	u.s	u.s	PROPN
ecletica-204	121	5	.	.	PROPN
ecletica-204	121	6	food	food	PROPN
ecletica-204	121	7	and	and	CCONJ
ecletica-204	121	8	drug	drug	NOUN
ecletica-204	121	9	administration	administration	NOUN
ecletica-204	121	10	.	.	PUNCT
ecletica-204	122	1	fda	fda	PROPN
ecletica-204	122	2	approves	approve	VERB
ecletica-204	122	3	new	new	ADJ
ecletica-204	122	4	treatment	treatment	NOUN
ecletica-204	122	5	for	for	ADP
ecletica-204	122	6	diabetes	diabetes	NOUN
ecletica-204	122	7	.	.	PUNCT
ecletica-204	123	1	2006	2006	NUM
ecletica-204	123	2	.	.	PUNCT
ecletica-204	124	1	[	[	X
ecletica-204	124	2	4	4	X
ecletica-204	124	3	]	]	X
ecletica-204	124	4	g.	g.	PROPN
ecletica-204	124	5	herman	herman	PROPN
ecletica-204	124	6	,	,	PUNCT
ecletica-204	124	7	a.	a.	PROPN
ecletica-204	124	8	bergman	bergman	PROPN
ecletica-204	124	9	,	,	PUNCT
ecletica-204	124	10	f.	f.	PROPN
ecletica-204	124	11	liu	liu	PROPN
ecletica-204	124	12	,	,	PUNCT
ecletica-204	124	13	c.	c.	PROPN
ecletica-204	124	14	stevens	stevens	PROPN
ecletica-204	124	15	,	,	PUNCT
ecletica-204	124	16	a.	a.	PROPN
ecletica-204	124	17	wang	wang	PROPN
ecletica-204	124	18	,	,	PUNCT
ecletica-204	124	19	w.	w.	PROPN
ecletica-204	124	20	zeng	zeng	PROPN
ecletica-204	124	21	,	,	PUNCT
ecletica-204	124	22	l.	l.	PROPN
ecletica-204	124	23	chen	chen	PROPN
ecletica-204	124	24	,	,	PUNCT
ecletica-204	124	25	k.	k.	PROPN
ecletica-204	124	26	snyder	snyder	PROPN
ecletica-204	124	27	,	,	PUNCT
ecletica-204	124	28	d.	d.	PROPN
ecletica-204	124	29	hilliard	hilliard	PROPN
ecletica-204	124	30	,	,	PUNCT
ecletica-204	124	31	m.	m.	NOUN
ecletica-204	124	32	tanen	tanen	NOUN
ecletica-204	124	33	,	,	PUNCT
ecletica-204	124	34	w.	w.	PROPN
ecletica-204	124	35	tanaka	tanaka	PROPN
ecletica-204	124	36	,	,	PUNCT
ecletica-204	124	37	a.	a.	NOUN
ecletica-204	124	38	meehan	meehan	PROPN
ecletica-204	124	39	,	,	PUNCT
ecletica-204	124	40	k.	k.	PROPN
ecletica-204	124	41	lasseter	lasseter	PROPN
ecletica-204	124	42	,	,	PUNCT
ecletica-204	124	43	s.	s.	PROPN
ecletica-204	124	44	dilzer	dilzer	PROPN
ecletica-204	124	45	,	,	PUNCT
ecletica-204	124	46	r.	r.	PROPN
ecletica-204	124	47	blum	blum	PROPN
ecletica-204	124	48	and	and	CCONJ
ecletica-204	124	49	j.	j.	PROPN
ecletica-204	124	50	wagner	wagner	PROPN
ecletica-204	124	51	.	.	PROPN
ecletica-204	124	52	journal	journal	PROPN
ecletica-204	124	53	of	of	ADP
ecletica-204	124	54	clinical	clinical	ADJ
ecletica-204	124	55	pharmacology	pharmacology	NOUN
ecletica-204	124	56	.	.	PUNCT
ecletica-204	125	1	46(8	46(8	NOUN
ecletica-204	125	2	)	)	PUNCT
ecletica-204	125	3	(	(	PUNCT
ecletica-204	125	4	2006	2006	NUM
ecletica-204	125	5	)	)	PUNCT
ecletica-204	125	6	876	876	NUM
ecletica-204	125	7	.	.	PUNCT
ecletica-204	126	1	[	[	X
ecletica-204	126	2	5	5	X
ecletica-204	126	3	]	]	PUNCT
ecletica-204	126	4	h.	h.	PROPN
ecletica-204	126	5	stella	stella	PROPN
ecletica-204	126	6	vincent	vincent	PROPN
ecletica-204	126	7	,	,	PUNCT
ecletica-204	126	8	r.	r.	PROPN
ecletica-204	126	9	james	james	PROPN
ecletica-204	126	10	reed	reed	PROPN
ecletica-204	126	11	,	,	PUNCT
ecletica-204	126	12	a.	a.	PROPN
ecletica-204	126	13	j.	j.	PROPN
ecletica-204	126	14	bergman	bergman	PROPN
ecletica-204	126	15	,	,	PUNCT
ecletica-204	126	16	c.	c.	PROPN
ecletica-204	126	17	s.	s.	PROPN
ecletica-204	126	18	elmore	elmore	PROPN
ecletica-204	126	19	,	,	PUNCT
ecletica-204	126	20	bing	bing	VERB
ecletica-204	126	21	zhu	zhu	PROPN
ecletica-204	126	22	,	,	PUNCT
ecletica-204	126	23	shiyao	shiyao	PROPN
ecletica-204	126	24	xu	xu	PROPN
ecletica-204	126	25	,	,	PUNCT
ecletica-204	126	26	david	david	PROPN
ecletica-204	126	27	ebel	ebel	PROPN
ecletica-204	126	28	,	,	PUNCT
ecletica-204	126	29	patrick	patrick	PROPN
ecletica-204	126	30	larson	larson	PROPN
ecletica-204	126	31	,	,	PUNCT
ecletica-204	126	32	wei	wei	PROPN
ecletica-204	126	33	zeng	zeng	PROPN
ecletica-204	126	34	,	,	PUNCT
ecletica-204	126	35	li	li	PROPN
ecletica-204	126	36	chen	chen	PROPN
ecletica-204	126	37	,	,	PUNCT
ecletica-204	126	38	stacy	stacy	PROPN
ecletica-204	126	39	dilzer	dilzer	PROPN
ecletica-204	126	40	,	,	PUNCT
ecletica-204	126	41	kenneth	kenneth	PROPN
ecletica-204	126	42	lasseter	lasseter	PROPN
ecletica-204	126	43	,	,	PUNCT
ecletica-204	126	44	keith	keith	PROPN
ecletica-204	126	45	gottesdiener	gottesdiener	PROPN
ecletica-204	126	46	,	,	PUNCT
ecletica-204	126	47	j.	j.	PROPN
ecletica-204	126	48	a.	a.	PROPN
ecletica-204	126	49	wagner	wagner	PROPN
ecletica-204	126	50	and	and	CCONJ
ecletica-204	126	51	g.	g.	PROPN
ecletica-204	126	52	a.	a.	PROPN
ecletica-204	126	53	herman	herman	PROPN
ecletica-204	126	54	.	.	PUNCT
ecletica-204	127	1	drug	drug	NOUN
ecletica-204	127	2	metabolism	metabolism	NOUN
ecletica-204	127	3	and	and	CCONJ
ecletica-204	127	4	disposition	disposition	NOUN
ecletica-204	127	5	.	.	PUNCT
ecletica-204	128	1	35(4	35(4	NUM
ecletica-204	128	2	)	)	PUNCT
ecletica-204	128	3	(	(	PUNCT
ecletica-204	128	4	2007	2007	NUM
ecletica-204	128	5	)	)	PUNCT
ecletica-204	128	6	533	533	NUM
ecletica-204	128	7	.	.	PUNCT
ecletica-204	129	1	[	[	X
ecletica-204	129	2	6	6	NUM
ecletica-204	129	3	]	]	PUNCT
ecletica-204	129	4	wei	wei	PROPN
ecletica-204	129	5	zeng	zeng	PROPN
ecletica-204	129	6	,	,	PUNCT
ecletica-204	129	7	donald	donald	PROPN
ecletica-204	129	8	g	g	PROPN
ecletica-204	129	9	musson	musson	PROPN
ecletica-204	129	10	,	,	PUNCT
ecletica-204	129	11	alison	alison	PROPN
ecletica-204	129	12	l	l	PROPN
ecletica-204	129	13	fisher	fisher	PROPN
ecletica-204	129	14	,	,	PUNCT
ecletica-204	129	15	li	li	PROPN
ecletica-204	129	16	chen	chen	PROPN
ecletica-204	129	17	,	,	PUNCT
ecletica-204	129	18	michael	michael	PROPN
ecletica-204	129	19	s	s	PROPN
ecletica-204	129	20	schwartz	schwartz	PROPN
ecletica-204	129	21	,	,	PUNCT
ecletica-204	129	22	eric	eric	PROPN
ecletica-204	129	23	j	j	PROPN
ecletica-204	129	24	woolf	woolf	PROPN
ecletica-204	129	25	and	and	CCONJ
ecletica-204	129	26	amy	amy	PROPN
ecletica-204	129	27	qiu	qiu	PROPN
ecletica-204	129	28	wang	wang	PROPN
ecletica-204	129	29	.	.	PUNCT
ecletica-204	130	1	journal	journal	PROPN
ecletica-204	130	2	of	of	ADP
ecletica-204	130	3	pharmaceutical	pharmaceutical	NOUN
ecletica-204	130	4	and	and	CCONJ
ecletica-204	130	5	biomedical	biomedical	ADJ
ecletica-204	130	6	analysis	analysis	NOUN
ecletica-204	130	7	.	.	PUNCT
ecletica-204	131	1	2008	2008	NUM
ecletica-204	131	2	;	;	PUNCT
ecletica-204	131	3	46(3	46(3	NUM
ecletica-204	131	4	)	)	PUNCT
ecletica-204	131	5	(	(	PUNCT
ecletica-204	131	6	2008	2008	NUM
ecletica-204	131	7	)	)	PUNCT
ecletica-204	131	8	534	534	NUM
ecletica-204	131	9	.	.	PUNCT
ecletica-204	132	1	[	[	X
ecletica-204	132	2	7	7	X
ecletica-204	132	3	]	]	PUNCT
ecletica-204	132	4	ramakrishna	ramakrishna	PROPN
ecletica-204	132	5	nirogi	nirogi	PROPN
ecletica-204	132	6	,	,	PUNCT
ecletica-204	132	7	vishwottam	vishwottam	PROPN
ecletica-204	132	8	kandikere	kandikere	PROPN
ecletica-204	132	9	,	,	PUNCT
ecletica-204	132	10	koteshwara	koteshwara	ADJ
ecletica-204	132	11	mudigonda	mudigonda	NOUN
ecletica-204	132	12	,	,	PUNCT
ecletica-204	132	13	prashanth	prashanth	PROPN
ecletica-204	132	14	komarneni	komarneni	NOUN
ecletica-204	132	15	,	,	PUNCT
ecletica-204	132	16	raghupathi	raghupathi	ADJ
ecletica-204	132	17	aleti	aleti	PROPN
ecletica-204	132	18	,	,	PUNCT
ecletica-204	132	19	rajeshkumar	rajeshkumar	PROPN
ecletica-204	132	20	boggavarapu	boggavarapu	PROPN
ecletica-204	132	21	.	.	PUNCT
ecletica-204	133	1	biomedical	biomedical	ADJ
ecletica-204	133	2	chromatography	chromatography	NOUN
ecletica-204	133	3	.	.	PUNCT
ecletica-204	134	1	22(2	22(2	VERB
ecletica-204	134	2	)	)	PUNCT
ecletica-204	134	3	(	(	PUNCT
ecletica-204	134	4	2008	2008	NUM
ecletica-204	134	5	)	)	PUNCT
ecletica-204	134	6	214	214	NUM
ecletica-204	134	7	.	.	PUNCT
ecletica-204	135	1	[	[	X
ecletica-204	135	2	8	8	NUM
ecletica-204	135	3	]	]	PUNCT
ecletica-204	135	4	m.	m.	NOUN
ecletica-204	135	5	g.	g.	PROPN
ecletica-204	135	6	beconi	beconi	PROPN
ecletica-204	135	7	,	,	PUNCT
ecletica-204	135	8	j.	j.	PROPN
ecletica-204	135	9	r.	r.	PROPN
ecletica-204	135	10	reed	reed	PROPN
ecletica-204	135	11	,	,	PUNCT
ecletica-204	135	12	yohannes	yohanne	NOUN
ecletica-204	135	13	teffera	teffera	NOUN
ecletica-204	135	14	,	,	PUNCT
ecletica-204	135	15	yuanqing	yuanqe	VERB
ecletica-204	135	16	xia	xia	PROPN
ecletica-204	135	17	,	,	PUNCT
ecletica-204	135	18	c.	c.	PROPN
ecletica-204	135	19	j.	j.	PROPN
ecletica-204	135	20	kochansky	kochansky	PROPN
ecletica-204	135	21	,	,	PUNCT
ecletica-204	135	22	d.	d.	PROPN
ecletica-204	135	23	q.	q.	PROPN
ecletica-204	135	24	liu	liu	PROPN
ecletica-204	135	25	,	,	PUNCT
ecletica-204	135	26	shiyao	shiyao	PROPN
ecletica-204	135	27	xu	xu	PROPN
ecletica-204	135	28	,	,	PUNCT
ecletica-204	135	29	c.	c.	PROPN
ecletica-204	135	30	s.	s.	PROPN
ecletica-204	135	31	elmore	elmore	PROPN
ecletica-204	135	32	,	,	PUNCT
ecletica-204	135	33	suzanne	suzanne	PROPN
ecletica-204	135	34	ciccotto	ciccotto	PROPN
ecletica-204	135	35	,	,	PUNCT
ecletica-204	135	36	d.	d.	PROPN
ecletica-204	135	37	f.	f.	PROPN
ecletica-204	135	38	hora	hora	PROPN
ecletica-204	135	39	,	,	PUNCT
ecletica-204	135	40	r.	r.	PROPN
ecletica-204	135	41	a.	a.	PROPN
ecletica-204	135	42	stearns	stearns	PROPN
ecletica-204	135	43	,	,	PUNCT
ecletica-204	135	44	and	and	CCONJ
ecletica-204	135	45	s.	s.	PROPN
ecletica-204	135	46	h.	h.	PROPN
ecletica-204	135	47	vincent	vincent	PROPN
ecletica-204	135	48	.	.	PUNCT
ecletica-204	136	1	drug	drug	NOUN
ecletica-204	136	2	metabolism	metabolism	NOUN
ecletica-204	136	3	and	and	CCONJ
ecletica-204	136	4	disposition	disposition	NOUN
ecletica-204	136	5	.	.	PUNCT
ecletica-204	137	1	35(4	35(4	NUM
ecletica-204	137	2	)	)	PUNCT
ecletica-204	137	3	(	(	PUNCT
ecletica-204	137	4	2007	2007	NUM
ecletica-204	137	5	)	)	PUNCT
ecletica-204	137	6	525	525	NUM
ecletica-204	137	7	.	.	PUNCT
ecletica-204	138	1	[	[	X
ecletica-204	138	2	9	9	NUM
ecletica-204	138	3	]	]	PUNCT
ecletica-204	138	4	f.	f.	PROPN
ecletica-204	138	5	r.	r.	PROPN
ecletica-204	138	6	s	s	PROPN
ecletica-204	138	7	derker	derker	PROPN
ecletica-204	138	8	bratlon	bratlon	PROPN
ecletica-204	138	9	and	and	CCONJ
ecletica-204	138	10	w.	w.	PROPN
ecletica-204	138	11	david	david	PROPN
ecletica-204	138	12	olis	olis	PROPN
ecletica-204	138	13	.	.	PUNCT
ecletica-204	139	1	comprehensive	comprehensive	ADJ
ecletica-204	139	2	organic	organic	ADJ
ecletica-204	139	3	chemistry	chemistry	NOUN
ecletica-204	139	4	,	,	PUNCT
ecletica-204	139	5	the	the	DET
ecletica-204	139	6	synthesis	synthesis	NOUN
ecletica-204	139	7	and	and	CCONJ
ecletica-204	139	8	reactions	reaction	NOUN
ecletica-204	139	9	of	of	ADP
ecletica-204	139	10	organic	organic	ADJ
ecletica-204	139	11	compounds	compound	NOUN
ecletica-204	139	12	.	.	PUNCT
ecletica-204	140	1	4	4	NUM
ecletica-204	140	2	,	,	PUNCT
ecletica-204	140	3	pergamon	pergamon	PROPN
ecletica-204	140	4	press	press	PROPN
ecletica-204	140	5	,	,	PUNCT
ecletica-204	140	6	london	london	PROPN
ecletica-204	140	7	,	,	PUNCT
ecletica-204	140	8	65	65	NUM
ecletica-204	140	9	,	,	PUNCT
ecletica-204	140	10	1979	1979	NUM
ecletica-204	140	11	,	,	PUNCT
ecletica-204	140	12	pp	pp	ADJ
ecletica-204	140	13	.	.	PUNCT
ecletica-204	141	1	298	298	NUM
ecletica-204	141	2	.	.	PUNCT
ecletica-204	142	1	[	[	X
ecletica-204	142	2	10	10	NUM
ecletica-204	142	3	]	]	PUNCT
ecletica-204	142	4	a.	a.	PROPN
ecletica-204	142	5	s.	s.	PROPN
ecletica-204	142	6	amin	amin	PROPN
ecletica-204	142	7	and	and	CCONJ
ecletica-204	142	8	m.	m.	NOUN
ecletica-204	142	9	m.	m.	NOUN
ecletica-204	142	10	zareh	zareh	PROPN
ecletica-204	142	11	.	.	PUNCT
ecletica-204	143	1	microchimica	microchimica	PROPN
ecletica-204	143	2	acta	acta	PROPN
ecletica-204	143	3	.	.	PROPN
ecletica-204	143	4	,	,	PUNCT
ecletica-204	143	5	124(3	124(3	NUM
ecletica-204	143	6	-	-	SYM
ecletica-204	143	7	4	4	NUM
ecletica-204	143	8	)	)	PUNCT
ecletica-204	143	9	(	(	PUNCT
ecletica-204	143	10	1996	1996	NUM
ecletica-204	143	11	)	)	PUNCT
ecletica-204	143	12	227	227	NUM
ecletica-204	143	13	.	.	PUNCT
ecletica-204	144	1	[	[	X
ecletica-204	144	2	11	11	NUM
ecletica-204	144	3	]	]	PUNCT
ecletica-204	144	4	a.	a.	PROPN
ecletica-204	144	5	s.	s.	PROPN
ecletica-204	144	6	ahmad	ahmad	PROPN
ecletica-204	144	7	,	,	PUNCT
ecletica-204	144	8	m.	m.	PROPN
ecletica-204	144	9	d.	d.	PROPN
ecletica-204	144	10	hoda	hoda	PROPN
ecletica-204	144	11	n	n	PROPN
ecletica-204	144	12	,	,	PUNCT
ecletica-204	144	13	m.	m.	PROPN
ecletica-204	144	14	ahmad	ahmad	PROPN
ecletica-204	144	15	,	,	PUNCT
ecletica-204	144	16	f.	f.	PROPN
ecletica-204	144	17	islam	islam	PROPN
ecletica-204	144	18	and	and	CCONJ
ecletica-204	144	19	s.	s.	PROPN
ecletica-204	144	20	z.	z.	PROPN
ecletica-204	144	21	qureshi	qureshi	PROPN
ecletica-204	144	22	.	.	PROPN
ecletica-204	145	1	journal	journal	PROPN
ecletica-204	145	2	of	of	ADP
ecletica-204	145	3	analytical	analytical	ADJ
ecletica-204	145	4	chemistry	chemistry	NOUN
ecletica-204	145	5	.	.	PUNCT
ecletica-204	146	1	61(9	61(9	NOUN
ecletica-204	146	2	)	)	PUNCT
ecletica-204	146	3	(	(	PUNCT
ecletica-204	146	4	2006	2006	NUM
ecletica-204	146	5	)	)	PUNCT
ecletica-204	146	6	870	870	NUM
ecletica-204	146	7	.	.	PUNCT
ecletica-204	147	1	[	[	X
ecletica-204	147	2	12	12	NUM
ecletica-204	147	3	]	]	PUNCT
ecletica-204	147	4	a.	a.	PROPN
ecletica-204	147	5	fawzy	fawzy	PROPN
ecletica-204	147	6	.	.	PUNCT
ecletica-204	148	1	el	el	PROPN
ecletica-204	148	2	-	-	PUNCT
ecletica-204	148	3	yazbi	yazbi	PROPN
ecletica-204	148	4	,	,	PUNCT
ecletica-204	148	5	h.	h.	PROPN
ecletica-204	148	6	h.	h.	PROPN
ecletica-204	148	7	abdine	abdine	PROPN
ecletica-204	148	8	and	and	CCONJ
ecletica-204	148	9	r.	r.	PROPN
ecletica-204	148	10	a.	a.	PROPN
ecletica-204	148	11	shaalan	shaalan	PROPN
ecletica-204	148	12	.	.	PUNCT
ecletica-204	149	1	journal	journal	PROPN
ecletica-204	149	2	of	of	ADP
ecletica-204	149	3	pharmaceutical	pharmaceutical	NOUN
ecletica-204	149	4	and	and	CCONJ
ecletica-204	149	5	biomedical	biomedical	ADJ
ecletica-204	149	6	analysis	analysis	NOUN
ecletica-204	149	7	.	.	PUNCT
ecletica-204	150	1	19(6	19(6	NUM
ecletica-204	150	2	)	)	PUNCT
ecletica-204	150	3	(	(	PUNCT
ecletica-204	150	4	1996	1996	NUM
ecletica-204	150	5	)	)	PUNCT
ecletica-204	150	6	819	819	NUM
ecletica-204	150	7	.	.	PUNCT
ecletica-204	151	1	[	[	X
ecletica-204	151	2	13	13	NUM
ecletica-204	151	3	]	]	PUNCT
ecletica-204	151	4	m.	m.	NOUN
ecletica-204	151	5	m.	m.	PROPN
ecletica-204	151	6	ayad	ayad	PROPN
ecletica-204	151	7	,	,	PUNCT
ecletica-204	151	8	m.	m.	NOUN
ecletica-204	151	9	m.	m.	PROPN
ecletica-204	151	10	el	el	PROPN
ecletica-204	151	11	-	-	PUNCT
ecletica-204	151	12	henawee	henawee	PROPN
ecletica-204	151	13	,	,	PUNCT
ecletica-204	151	14	h.	h.	PROPN
ecletica-204	151	15	e.	e.	PROPN
ecletica-204	151	16	abdellatef	abdellatef	PROPN
ecletica-204	151	17	,	,	PUNCT
ecletica-204	151	18	h.	h.	PROPN
ecletica-204	151	19	m.	m.	PROPN
ecletica-204	151	20	el	el	PROPN
ecletica-204	151	21	-	-	PUNCT
ecletica-204	151	22	sayed	say	VERB
ecletica-204	151	23	.	.	PUNCT
ecletica-204	152	1	alexandria	alexandria	PROPN
ecletica-204	152	2	journal	journal	PROPN
ecletica-204	152	3	of	of	ADP
ecletica-204	152	4	pharmaceutical	pharmaceutical	NOUN
ecletica-204	152	5	sciences	science	NOUN
ecletica-204	152	6	.	.	PUNCT
ecletica-204	153	1	9(2	9(2	NUM
ecletica-204	153	2	)	)	PUNCT
ecletica-204	153	3	(	(	PUNCT
ecletica-204	153	4	2005	2005	NUM
ecletica-204	153	5	)	)	PUNCT
ecletica-204	153	6	157	157	NUM
ecletica-204	153	7	.	.	PUNCT
ecletica-204	154	1	[	[	X
ecletica-204	154	2	14	14	NUM
ecletica-204	154	3	]	]	PUNCT
ecletica-204	154	4	khalifa	khalifa	PROPN
ecletica-204	154	5	abulghasem	abulghasem	PROPN
ecletica-204	154	6	el	el	PROPN
ecletica-204	154	7	-	-	PUNCT
ecletica-204	154	8	aroud	aroud	NOUN
ecletica-204	154	9	,	,	PUNCT
ecletica-204	154	10	adel	adel	PROPN
ecletica-204	154	11	mohamed	mohamed	PROPN
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ecletica-204	154	13	and	and	CCONJ
ecletica-204	154	14	hisham	hisham	PROPN
ecletica-204	154	15	ezzat	ezzat	PROPN
ecletica-204	154	16	abdellatef	abdellatef	PROPN
ecletica-204	154	17	.	.	PUNCT
ecletica-204	155	1	chem	chem	PROPN
ecletica-204	155	2	.	.	PUNCT
ecletica-204	156	1	pharm	pharm	NOUN
ecletica-204	156	2	.	.	PUNCT
ecletica-204	157	1	bull	bull	NOUN
ecletica-204	157	2	.	.	PUNCT
ecletica-204	158	1	55(3	55(3	X
ecletica-204	158	2	)	)	PUNCT
ecletica-204	158	3	(	(	PUNCT
ecletica-204	158	4	2007	2007	NUM
ecletica-204	158	5	)	)	PUNCT
ecletica-204	158	6	364	364	NUM
ecletica-204	158	7	.	.	PUNCT
ecletica-204	159	1	[	[	X
ecletica-204	159	2	15	15	NUM
ecletica-204	159	3	]	]	X
ecletica-204	159	4	analytical	analytical	ADJ
ecletica-204	159	5	methods	method	NOUN
ecletica-204	159	6	committee	committee	PROPN
ecletica-204	159	7	,	,	PUNCT
ecletica-204	159	8	1987	1987	NUM
ecletica-204	159	9	.	.	PUNCT
ecletica-204	160	1	recommendations	recommendation	NOUN
ecletica-204	160	2	for	for	ADP
ecletica-204	160	3	the	the	DET
ecletica-204	160	4	definition	definition	NOUN
ecletica-204	160	5	,	,	PUNCT
ecletica-204	160	6	estimation	estimation	NOUN
ecletica-204	160	7	and	and	CCONJ
ecletica-204	160	8	use	use	NOUN
ecletica-204	160	9	of	of	ADP
ecletica-204	160	10	the	the	DET
ecletica-204	160	11	detection	detection	NOUN
ecletica-204	160	12	limit	limit	NOUN
ecletica-204	160	13	.	.	PUNCT
ecletica-204	161	1	1987	1987	NUM
ecletica-204	161	2	.	.	PUNCT
ecletica-204	162	1	analyst	analyst	NOUN
ecletica-204	162	2	.	.	PUNCT
ecletica-204	162	3	,	,	PUNCT
ecletica-204	163	1	pp:199	pp:199	X
ecletica-204	163	2	[	[	X
ecletica-204	163	3	16	16	NUM
ecletica-204	163	4	]	]	PUNCT
ecletica-204	163	5	h.	h.	PROPN
ecletica-204	163	6	f.	f.	PROPN
ecletica-204	163	7	askal	askal	PROPN
ecletica-204	163	8	,	,	PUNCT
ecletica-204	163	9	g.	g.	PROPN
ecletica-204	163	10	a.	a.	PROPN
ecletica-204	163	11	saleh	saleh	PROPN
ecletica-204	163	12	,	,	PUNCT
ecletica-204	163	13	n.	n.	PROPN
ecletica-204	163	14	m.	m.	PROPN
ecletica-204	163	15	omar	omar	PROPN
ecletica-204	163	16	,	,	PUNCT
ecletica-204	163	17	analyst	analyst	NOUN
ecletica-204	163	18	,	,	PUNCT
ecletica-204	163	19	116(4	116(4	NUM
ecletica-204	163	20	)	)	PUNCT
ecletica-204	163	21	(	(	PUNCT
ecletica-204	163	22	1991	1991	NUM
ecletica-204	163	23	)	)	PUNCT
ecletica-204	163	24	387	387	NUM
ecletica-204	163	25	.	.	PUNCT