id	sid	tid	token	lemma	pos
ecletica-56	1	1	1	1	NUM
ecletica-56	1	2	eclética	eclética	NOUN
ecletica-56	1	3	química	química	PROPN
ecletica-56	1	4	original	original	ADJ
ecletica-56	1	5	research	research	NOUN
ecletica-56	1	6	publication	publication	NOUN
ecletica-56	1	7	in	in	ADP
ecletica-56	1	8	all	all	DET
ecletica-56	1	9	aspects	aspect	NOUN
ecletica-56	1	10	of	of	ADP
ecletica-56	1	11	chemistry	chemistry	NOUN
ecletica-56	1	12	homepage	homepage	NOUN
ecletica-56	1	13	:	:	PUNCT
ecletica-56	1	14	www.iq.unesp.br/ecletica	www.iq.unesp.br/ecletica	PROPN
ecletica-56	1	15	issn	issn	PROPN
ecletica-56	1	16	1678	1678	NUM
ecletica-56	1	17	-	-	SYM
ecletica-56	1	18	4618	4618	NUM
ecletica-56	1	19	|	|	NOUN
ecletica-56	1	20	vol	vol	NOUN
ecletica-56	1	21	.	.	PROPN
ecletica-56	2	1	40	40	NUM
ecletica-56	3	1	|	|	ADV
ecletica-56	3	2	2015	2015	NUM
ecletica-56	3	3	|	|	ADV
ecletica-56	3	4	artigo	artigo	PROPN
ecletica-56	3	5	06	06	NUM
ecletica-56	4	1	|	|	ADV
ecletica-56	4	2	eclética	eclética	PROPN
ecletica-56	4	3	química	química	PROPN
ecletica-56	4	4	,	,	PUNCT
ecletica-56	4	5	vol	vol	NOUN
ecletica-56	4	6	.	.	PROPN
ecletica-56	4	7	40	40	NUM
ecletica-56	4	8	,	,	PUNCT
ecletica-56	4	9	62	62	NUM
ecletica-56	4	10	-	-	SYM
ecletica-56	4	11	70	70	NUM
ecletica-56	4	12	,	,	PUNCT
ecletica-56	4	13	2015	2015	NUM
ecletica-56	4	14	.	.	PUNCT
ecletica-56	5	1	62	62	NUM
ecletica-56	5	2	microgravimetric	microgravimetric	ADJ
ecletica-56	5	3	method	method	NOUN
ecletica-56	5	4	for	for	ADP
ecletica-56	5	5	the	the	DET
ecletica-56	5	6	determination	determination	NOUN
ecletica-56	5	7	of	of	ADP
ecletica-56	5	8	metformin	metformin	NOUN
ecletica-56	5	9	in	in	ADP
ecletica-56	5	10	pharmaceutical	pharmaceutical	ADJ
ecletica-56	5	11	preparations	preparation	NOUN
ecletica-56	5	12	and	and	CCONJ
ecletica-56	5	13	in	in	ADP
ecletica-56	5	14	the	the	DET
ecletica-56	5	15	bulk	bulk	ADJ
ecletica-56	5	16	drug	drug	NOUN
ecletica-56	5	17	matthieu	matthieu	PROPN
ecletica-56	5	18	tubino	tubino	VERB
ecletica-56	5	19	1	1	NUM
ecletica-56	5	20	,	,	PUNCT
ecletica-56	5	21	luís	luís	PROPN
ecletica-56	5	22	francisco	francisco	PROPN
ecletica-56	5	23	bianchessi	bianchessi	PROPN
ecletica-56	5	24	1	1	NUM
ecletica-56	5	25	,	,	PUNCT
ecletica-56	5	26	marta	marta	PROPN
ecletica-56	5	27	m.	m.	PROPN
ecletica-56	5	28	d.	d.	PROPN
ecletica-56	5	29	c.	c.	PROPN
ecletica-56	5	30	vila	vila	PROPN
ecletica-56	6	1	2	2	NUM
ecletica-56	6	2	_	_	PUNCT
ecletica-56	7	1	_	_	PUNCT
ecletica-56	8	1	_	_	PUNCT
ecletica-56	9	1	_	_	PUNCT
ecletica-56	10	1	_	_	PUNCT
ecletica-56	11	1	_	_	PUNCT
ecletica-56	12	1	_	_	PUNCT
ecletica-56	13	1	_	_	PUNCT
ecletica-56	14	1	_	_	PUNCT
ecletica-56	15	1	_	_	PUNCT
ecletica-56	16	1	_	_	PUNCT
ecletica-56	17	1	_	_	PUNCT
ecletica-56	18	1	_	_	PUNCT
ecletica-56	19	1	_	_	PUNCT
ecletica-56	20	1	_	_	PUNCT
ecletica-56	21	1	_	_	PUNCT
ecletica-56	22	1	_	_	PUNCT
ecletica-56	23	1	_	_	PUNCT
ecletica-56	24	1	_	_	PUNCT
ecletica-56	25	1	_	_	PUNCT
ecletica-56	26	1	_	_	PUNCT
ecletica-56	27	1	_	_	PUNCT
ecletica-56	28	1	_	_	PUNCT
ecletica-56	29	1	_	_	PUNCT
ecletica-56	30	1	_	_	PUNCT
ecletica-56	31	1	_	_	PUNCT
ecletica-56	32	1	_	_	PUNCT
ecletica-56	33	1	_	_	PUNCT
ecletica-56	34	1	_	_	PUNCT
ecletica-56	35	1	_	_	PUNCT
ecletica-56	36	1	_	_	PUNCT
ecletica-56	37	1	_	_	PUNCT
ecletica-56	38	1	_	_	PUNCT
ecletica-56	39	1	_	_	PUNCT
ecletica-56	40	1	_	_	PUNCT
ecletica-56	41	1	_	_	PUNCT
ecletica-56	42	1	_	_	PUNCT
ecletica-56	43	1	_	_	PUNCT
ecletica-56	44	1	_	_	PUNCT
ecletica-56	45	1	_	_	PUNCT
ecletica-56	46	1	_	_	PUNCT
ecletica-56	47	1	_	_	PUNCT
ecletica-56	48	1	_	_	PUNCT
ecletica-56	49	1	_	_	PUNCT
ecletica-56	50	1	_	_	PUNCT
ecletica-56	51	1	_	_	PUNCT
ecletica-56	52	1	_	_	PUNCT
ecletica-56	53	1	_	_	PUNCT
ecletica-56	54	1	_	_	PUNCT
ecletica-56	55	1	_	_	PUNCT
ecletica-56	56	1	_	_	PUNCT
ecletica-56	57	1	_	_	PUNCT
ecletica-56	58	1	_	_	PUNCT
ecletica-56	59	1	_	_	PUNCT
ecletica-56	60	1	_	_	PUNCT
ecletica-56	61	1	_	_	PUNCT
ecletica-56	62	1	_	_	PUNCT
ecletica-56	63	1	_	_	PUNCT
ecletica-56	64	1	_	_	PUNCT
ecletica-56	65	1	_	_	PUNCT
ecletica-56	66	1	_	_	PUNCT
ecletica-56	67	1	_	_	PUNCT
ecletica-56	68	1	_	_	PUNCT
ecletica-56	69	1	_	_	PUNCT
ecletica-56	70	1	_	_	PUNCT
ecletica-56	71	1	_	_	PUNCT
ecletica-56	72	1	_	_	PUNCT
ecletica-56	73	1	_	_	PUNCT
ecletica-56	74	1	_	_	PUNCT
ecletica-56	75	1	_	_	PUNCT
ecletica-56	76	1	_	_	PUNCT
ecletica-56	77	1	_	_	PUNCT
ecletica-56	78	1	_	_	PUNCT
ecletica-56	79	1	_	_	PUNCT
ecletica-56	80	1	_	_	PUNCT
ecletica-56	81	1	_	_	PUNCT
ecletica-56	82	1	abstract	abstract	ADJ
ecletica-56	82	2	:	:	PUNCT
ecletica-56	82	3	this	this	DET
ecletica-56	82	4	article	article	NOUN
ecletica-56	82	5	reports	report	VERB
ecletica-56	82	6	a	a	DET
ecletica-56	82	7	microgravimetric	microgravimetric	ADJ
ecletica-56	82	8	method	method	NOUN
ecletica-56	82	9	for	for	ADP
ecletica-56	82	10	the	the	DET
ecletica-56	82	11	quantitative	quantitative	ADJ
ecletica-56	82	12	determination	determination	NOUN
ecletica-56	82	13	of	of	ADP
ecletica-56	82	14	metformin	metformin	NOUN
ecletica-56	82	15	in	in	ADP
ecletica-56	82	16	bulk	bulk	NOUN
ecletica-56	82	17	and	and	CCONJ
ecletica-56	82	18	in	in	ADP
ecletica-56	82	19	pharmaceutical	pharmaceutical	ADJ
ecletica-56	82	20	preparations	preparation	NOUN
ecletica-56	82	21	.	.	PUNCT
ecletica-56	83	1	the	the	DET
ecletica-56	83	2	analysis	analysis	NOUN
ecletica-56	83	3	is	be	AUX
ecletica-56	83	4	simple	simple	ADJ
ecletica-56	83	5	and	and	CCONJ
ecletica-56	83	6	relatively	relatively	ADV
ecletica-56	83	7	rapid	rapid	ADJ
ecletica-56	83	8	.	.	PUNCT
ecletica-56	84	1	a	a	DET
ecletica-56	84	2	complete	complete	ADJ
ecletica-56	84	3	analysis	analysis	NOUN
ecletica-56	84	4	can	can	AUX
ecletica-56	84	5	be	be	AUX
ecletica-56	84	6	performed	perform	VERB
ecletica-56	84	7	in	in	ADP
ecletica-56	84	8	only	only	ADV
ecletica-56	84	9	an	an	DET
ecletica-56	84	10	hour	hour	NOUN
ecletica-56	84	11	and	and	CCONJ
ecletica-56	84	12	thirty	thirty	NUM
ecletica-56	84	13	minutes	minute	NOUN
ecletica-56	84	14	due	due	ADP
ecletica-56	84	15	to	to	ADP
ecletica-56	84	16	the	the	DET
ecletica-56	84	17	drying	dry	VERB
ecletica-56	84	18	procedure	procedure	NOUN
ecletica-56	84	19	of	of	ADP
ecletica-56	84	20	the	the	DET
ecletica-56	84	21	precipitate	precipitate	NOUN
ecletica-56	84	22	.	.	PUNCT
ecletica-56	85	1	however	however	ADV
ecletica-56	85	2	a	a	DET
ecletica-56	85	3	sample	sample	NOUN
ecletica-56	85	4	can	can	AUX
ecletica-56	85	5	be	be	AUX
ecletica-56	85	6	treated	treat	VERB
ecletica-56	85	7	every	every	DET
ecletica-56	85	8	each	each	DET
ecletica-56	85	9	five	five	NUM
ecletica-56	85	10	minutes	minute	NOUN
ecletica-56	85	11	.	.	PUNCT
ecletica-56	86	1	the	the	DET
ecletica-56	86	2	method	method	NOUN
ecletica-56	86	3	is	be	AUX
ecletica-56	86	4	based	base	VERB
ecletica-56	86	5	on	on	ADP
ecletica-56	86	6	the	the	DET
ecletica-56	86	7	reaction	reaction	NOUN
ecletica-56	86	8	of	of	ADP
ecletica-56	86	9	nickel	nickel	NOUN
ecletica-56	86	10	(	(	PUNCT
ecletica-56	86	11	ii	ii	NOUN
ecletica-56	86	12	)	)	PUNCT
ecletica-56	86	13	with	with	ADP
ecletica-56	86	14	metformin	metformin	NOUN
ecletica-56	86	15	that	that	SCONJ
ecletica-56	86	16	in	in	ADP
ecletica-56	86	17	basic	basic	ADJ
ecletica-56	86	18	medium	medium	ADJ
ecletica-56	86	19	forms	form	NOUN
ecletica-56	86	20	an	an	DET
ecletica-56	86	21	orange	orange	ADJ
ecletica-56	86	22	precipitate	precipitate	NOUN
ecletica-56	86	23	.	.	PUNCT
ecletica-56	87	1	the	the	DET
ecletica-56	87	2	reaction	reaction	NOUN
ecletica-56	87	3	is	be	AUX
ecletica-56	87	4	performed	perform	VERB
ecletica-56	87	5	in	in	ADP
ecletica-56	87	6	a	a	DET
ecletica-56	87	7	plastic	plastic	ADJ
ecletica-56	87	8	syringe	syringe	NOUN
ecletica-56	87	9	.	.	PUNCT
ecletica-56	88	1	the	the	DET
ecletica-56	88	2	filtration	filtration	NOUN
ecletica-56	88	3	was	be	AUX
ecletica-56	88	4	done	do	VERB
ecletica-56	88	5	in	in	ADP
ecletica-56	88	6	a	a	DET
ecletica-56	88	7	glass	glass	NOUN
ecletica-56	88	8	tube	tube	NOUN
ecletica-56	88	9	containing	contain	VERB
ecletica-56	88	10	a	a	DET
ecletica-56	88	11	sintered	sinter	VERB
ecletica-56	88	12	glass	glass	NOUN
ecletica-56	88	13	disk	disk	NOUN
ecletica-56	88	14	or	or	CCONJ
ecletica-56	88	15	in	in	ADP
ecletica-56	88	16	millipore	millipore	NOUN
ecletica-56	88	17	®	®	NOUN
ecletica-56	88	18	syringe	syringe	NOUN
ecletica-56	88	19	filters	filter	NOUN
ecletica-56	88	20	,	,	PUNCT
ecletica-56	88	21	with	with	ADP
ecletica-56	88	22	posterior	posterior	ADJ
ecletica-56	88	23	weighing	weigh	VERB
ecletica-56	88	24	after	after	ADP
ecletica-56	88	25	drying	dry	VERB
ecletica-56	88	26	.	.	PUNCT
ecletica-56	89	1	the	the	DET
ecletica-56	89	2	analytical	analytical	ADJ
ecletica-56	89	3	results	result	NOUN
ecletica-56	89	4	were	be	AUX
ecletica-56	89	5	statistically	statistically	ADV
ecletica-56	89	6	compared	compare	VERB
ecletica-56	89	7	with	with	ADP
ecletica-56	89	8	that	that	PRON
ecletica-56	89	9	obtained	obtain	VERB
ecletica-56	89	10	with	with	ADP
ecletica-56	89	11	a	a	DET
ecletica-56	89	12	hplc	hplc	NOUN
ecletica-56	89	13	and	and	CCONJ
ecletica-56	89	14	with	with	ADP
ecletica-56	89	15	the	the	DET
ecletica-56	89	16	titrimetric	titrimetric	ADJ
ecletica-56	89	17	method	method	NOUN
ecletica-56	89	18	suggested	suggest	VERB
ecletica-56	89	19	by	by	ADP
ecletica-56	89	20	the	the	DET
ecletica-56	89	21	united	united	PROPN
ecletica-56	89	22	states	states	PROPN
ecletica-56	89	23	and	and	CCONJ
ecletica-56	89	24	by	by	ADP
ecletica-56	89	25	the	the	DET
ecletica-56	89	26	japanese	japanese	ADJ
ecletica-56	89	27	pharmacopoeias	pharmacopoeia	NOUN
ecletica-56	89	28	.	.	PUNCT
ecletica-56	90	1	keywords	keyword	NOUN
ecletica-56	90	2	:	:	PUNCT
ecletica-56	90	3	metformin	metformin	NOUN
ecletica-56	90	4	;	;	PUNCT
ecletica-56	90	5	microgravimetry	microgravimetry	NOUN
ecletica-56	90	6	;	;	PUNCT
ecletica-56	90	7	nickel	nickel	NOUN
ecletica-56	90	8	complex	complex	NOUN
ecletica-56	90	9	;	;	PUNCT
ecletica-56	90	10	analysis	analysis	NOUN
ecletica-56	90	11	;	;	PUNCT
ecletica-56	90	12	syringe	syringe	NOUN
ecletica-56	90	13	filters	filter	NOUN
ecletica-56	90	14	1	1	NUM
ecletica-56	90	15	institute	institute	NOUN
ecletica-56	90	16	of	of	ADP
ecletica-56	90	17	chemistry	chemistry	NOUN
ecletica-56	90	18	,	,	PUNCT
ecletica-56	90	19	university	university	PROPN
ecletica-56	90	20	of	of	ADP
ecletica-56	90	21	campinas	campinas	PROPN
ecletica-56	90	22	,	,	PUNCT
ecletica-56	90	23	campinas	campinas	PROPN
ecletica-56	90	24	,	,	PUNCT
ecletica-56	90	25	sp	sp	PROPN
ecletica-56	90	26	,	,	PUNCT
ecletica-56	90	27	brazil	brazil	PROPN
ecletica-56	90	28	13083	13083	NUM
ecletica-56	90	29	-	-	SYM
ecletica-56	90	30	970	970	NUM
ecletica-56	90	31	p.o	p.o	PROPN
ecletica-56	90	32	.	.	PROPN
ecletica-56	90	33	box	box	PROPN
ecletica-56	90	34	6154	6154	NUM
ecletica-56	90	35	2	2	NUM
ecletica-56	90	36	university	university	NOUN
ecletica-56	90	37	of	of	ADP
ecletica-56	90	38	sorocaba	sorocaba	PROPN
ecletica-56	90	39	,	,	PUNCT
ecletica-56	90	40	sorocaba	sorocaba	PROPN
ecletica-56	90	41	,	,	PUNCT
ecletica-56	90	42	sp	sp	NOUN
ecletica-56	90	43	,	,	PUNCT
ecletica-56	90	44	brazil	brazil	PROPN
ecletica-56	90	45	13087	13087	NUM
ecletica-56	90	46	-	-	PUNCT
ecletica-56	90	47	000	000	NUM
ecletica-56	90	48	file:///c:/users	file:///c:/users	PROPN
ecletica-56	90	49	/	/	SYM
ecletica-56	90	50	catia	catia	NOUN
ecletica-56	90	51	/	/	SYM
ecletica-56	90	52	desktop	desktop	NOUN
ecletica-56	90	53	/	/	SYM
ecletica-56	90	54	eclética%20vol%2040	eclética%20vol%2040	NOUN
ecletica-56	90	55	/	/	SYM
ecletica-56	90	56	nova%20pasta	nova%20pasta	NOUN
ecletica-56	90	57	/	/	SYM
ecletica-56	90	58	www.iq.unesp.br	www.iq.unesp.br	NOUN
ecletica-56	90	59	/	/	SYM
ecletica-56	90	60	ecletica	ecletica	NOUN
ecletica-56	90	61	eclética	eclética	PROPN
ecletica-56	90	62	química	química	PROPN
ecletica-56	90	63	,	,	PUNCT
ecletica-56	90	64	vol	vol	NOUN
ecletica-56	90	65	.	.	PROPN
ecletica-56	90	66	40	40	NUM
ecletica-56	90	67	,	,	PUNCT
ecletica-56	90	68	62	62	NUM
ecletica-56	90	69	-	-	SYM
ecletica-56	90	70	70	70	NUM
ecletica-56	90	71	,	,	PUNCT
ecletica-56	90	72	2015	2015	NUM
ecletica-56	90	73	.	.	PUNCT
ecletica-56	91	1	63	63	NUM
ecletica-56	91	2	63	63	NUM
ecletica-56	91	3	introduction	introduction	NOUN
ecletica-56	91	4	diabetes	diabetes	NOUN
ecletica-56	91	5	mellitus	mellitus	NOUN
ecletica-56	91	6	(	(	PUNCT
ecletica-56	91	7	dm	dm	PROPN
ecletica-56	91	8	)	)	PUNCT
ecletica-56	91	9	is	be	AUX
ecletica-56	91	10	a	a	DET
ecletica-56	91	11	heterogeneous	heterogeneous	ADJ
ecletica-56	91	12	syndrome	syndrome	NOUN
ecletica-56	91	13	characterized	characterize	VERB
ecletica-56	91	14	by	by	ADP
ecletica-56	91	15	endocrine	endocrine	NOUN
ecletica-56	91	16	-	-	PUNCT
ecletica-56	91	17	metabolic	metabolic	NOUN
ecletica-56	91	18	abnormalities	abnormality	NOUN
ecletica-56	91	19	that	that	PRON
ecletica-56	91	20	modify	modify	VERB
ecletica-56	91	21	the	the	DET
ecletica-56	91	22	metabolic	metabolic	NOUN
ecletica-56	91	23	homeostasis	homeostasis	NOUN
ecletica-56	91	24	in	in	ADP
ecletica-56	91	25	humans	human	NOUN
ecletica-56	91	26	[	[	X
ecletica-56	91	27	1	1	NUM
ecletica-56	91	28	]	]	PUNCT
ecletica-56	91	29	.	.	PUNCT
ecletica-56	92	1	this	this	DET
ecletica-56	92	2	pathology	pathology	NOUN
ecletica-56	92	3	has	have	AUX
ecletica-56	92	4	been	be	AUX
ecletica-56	92	5	in	in	ADP
ecletica-56	92	6	continuous	continuous	ADJ
ecletica-56	92	7	increasing	increasing	NOUN
ecletica-56	92	8	and	and	CCONJ
ecletica-56	92	9	among	among	ADP
ecletica-56	92	10	the	the	DET
ecletica-56	92	11	chronicle	chronicle	PROPN
ecletica-56	92	12	non	non	ADJ
ecletica-56	92	13	transmissible	transmissible	ADJ
ecletica-56	92	14	diseases	disease	NOUN
ecletica-56	92	15	it	it	PRON
ecletica-56	92	16	is	be	AUX
ecletica-56	92	17	one	one	NUM
ecletica-56	92	18	of	of	ADP
ecletica-56	92	19	the	the	DET
ecletica-56	92	20	more	more	ADV
ecletica-56	92	21	relevant	relevant	ADJ
ecletica-56	93	1	[	[	X
ecletica-56	93	2	2	2	NUM
ecletica-56	93	3	]	]	PUNCT
ecletica-56	93	4	.	.	PUNCT
ecletica-56	94	1	metformin	metformin	NOUN
ecletica-56	94	2	(	(	PUNCT
ecletica-56	94	3	1,1	1,1	NUM
ecletica-56	94	4	-	-	PUNCT
ecletica-56	94	5	dimethylbiguanidine	dimethylbiguanidine	NOUN
ecletica-56	94	6	)	)	PUNCT
ecletica-56	94	7	is	be	AUX
ecletica-56	94	8	an	an	DET
ecletica-56	94	9	hypoglycemiant	hypoglycemiant	NOUN
ecletica-56	94	10	agent	agent	NOUN
ecletica-56	94	11	employed	employ	VERB
ecletica-56	94	12	in	in	ADP
ecletica-56	94	13	type	type	NOUN
ecletica-56	94	14	2	2	NUM
ecletica-56	94	15	diabetes	diabetes	NOUN
ecletica-56	94	16	mellitus	mellitus	NOUN
ecletica-56	94	17	(	(	PUNCT
ecletica-56	94	18	dm2)[3	dm2)[3	ADJ
ecletica-56	94	19	]	]	PUNCT
ecletica-56	94	20	.	.	PUNCT
ecletica-56	95	1	it	it	PRON
ecletica-56	95	2	is	be	AUX
ecletica-56	95	3	usually	usually	ADV
ecletica-56	95	4	found	find	VERB
ecletica-56	95	5	in	in	ADP
ecletica-56	95	6	the	the	DET
ecletica-56	95	7	hydrochloride	hydrochloride	NOUN
ecletica-56	95	8	in	in	ADP
ecletica-56	95	9	500	500	NUM
ecletica-56	95	10	mg	mg	NOUN
ecletica-56	95	11	and	and	CCONJ
ecletica-56	95	12	850	850	NUM
ecletica-56	95	13	mg	mg	PROPN
ecletica-56	95	14	tablets	tablet	NOUN
ecletica-56	95	15	.	.	PUNCT
ecletica-56	96	1	metformin	metformin	NOUN
ecletica-56	96	2	chloridrate	chloridrate	PROPN
ecletica-56	96	3	is	be	AUX
ecletica-56	96	4	a	a	DET
ecletica-56	96	5	white	white	ADJ
ecletica-56	96	6	crystalline	crystalline	NOUN
ecletica-56	96	7	solid	solid	ADJ
ecletica-56	96	8	.	.	PUNCT
ecletica-56	97	1	its	its	PRON
ecletica-56	97	2	molecular	molecular	ADJ
ecletica-56	97	3	formula	formula	NOUN
ecletica-56	97	4	is	be	AUX
ecletica-56	97	5	c4h11n5·hcl	c4h11n5·hcl	PROPN
ecletica-56	97	6	(	(	PUNCT
ecletica-56	97	7	fig	fig	NOUN
ecletica-56	97	8	.	.	NOUN
ecletica-56	97	9	1	1	NUM
ecletica-56	97	10	)	)	PUNCT
ecletica-56	97	11	and	and	CCONJ
ecletica-56	97	12	the	the	DET
ecletica-56	97	13	molecular	molecular	ADJ
ecletica-56	97	14	mass	mass	NOUN
ecletica-56	97	15	165.63	165.63	NUM
ecletica-56	97	16	da	da	NOUN
ecletica-56	97	17	.	.	PUNCT
ecletica-56	97	18	is	be	AUX
ecletica-56	97	19	freely	freely	ADV
ecletica-56	97	20	soluble	soluble	ADJ
ecletica-56	97	21	in	in	ADP
ecletica-56	97	22	water	water	NOUN
ecletica-56	97	23	but	but	CCONJ
ecletica-56	97	24	insoluble	insoluble	ADJ
ecletica-56	97	25	in	in	ADP
ecletica-56	97	26	acetone	acetone	NOUN
ecletica-56	97	27	,	,	PUNCT
ecletica-56	97	28	ether	ether	NOUN
ecletica-56	97	29	and	and	CCONJ
ecletica-56	97	30	chloroform	chloroform	NOUN
ecletica-56	98	1	[	[	X
ecletica-56	98	2	4,5	4,5	NUM
ecletica-56	98	3	]	]	PUNCT
ecletica-56	98	4	.	.	PUNCT
ecletica-56	99	1	figure	figure	VERB
ecletica-56	99	2	1	1	NUM
ecletica-56	99	3	some	some	DET
ecletica-56	99	4	analytical	analytical	ADJ
ecletica-56	99	5	procedures	procedure	NOUN
ecletica-56	99	6	are	be	AUX
ecletica-56	99	7	reported	report	VERB
ecletica-56	99	8	in	in	ADP
ecletica-56	99	9	the	the	DET
ecletica-56	99	10	literature	literature	NOUN
ecletica-56	99	11	for	for	ADP
ecletica-56	99	12	the	the	DET
ecletica-56	99	13	determination	determination	NOUN
ecletica-56	99	14	of	of	ADP
ecletica-56	99	15	metformin[6,7	metformin[6,7	PROPN
ecletica-56	99	16	]	]	PUNCT
ecletica-56	99	17	.	.	PUNCT
ecletica-56	100	1	an	an	DET
ecletica-56	100	2	official	official	ADJ
ecletica-56	100	3	analytical	analytical	ADJ
ecletica-56	100	4	method	method	NOUN
ecletica-56	100	5	of	of	ADP
ecletica-56	100	6	metformin	metformin	NOUN
ecletica-56	100	7	chloridrate	chloridrate	NOUN
ecletica-56	100	8	indicated	indicate	VERB
ecletica-56	100	9	in	in	ADP
ecletica-56	100	10	various	various	ADJ
ecletica-56	100	11	pharmacopoeias	pharmacopoeia	NOUN
ecletica-56	100	12	is	be	AUX
ecletica-56	100	13	the	the	DET
ecletica-56	100	14	potentiometric	potentiometric	ADJ
ecletica-56	100	15	titration	titration	NOUN
ecletica-56	100	16	in	in	ADP
ecletica-56	100	17	non	non	ADJ
ecletica-56	100	18	aqueous	aqueous	ADJ
ecletica-56	100	19	solution[8	solution[8	NOUN
ecletica-56	100	20	-	-	SYM
ecletica-56	100	21	11	11	NUM
ecletica-56	100	22	]	]	PUNCT
ecletica-56	100	23	.	.	PUNCT
ecletica-56	101	1	conductimetric	conductimetric	ADJ
ecletica-56	101	2	titrations	titration	NOUN
ecletica-56	101	3	are	be	AUX
ecletica-56	101	4	proposed	propose	VERB
ecletica-56	101	5	by	by	ADP
ecletica-56	101	6	abou	abou	PROPN
ecletica-56	101	7	-	-	PUNCT
ecletica-56	101	8	dan	dan	PROPN
ecletica-56	101	9	et	et	PROPN
ecletica-56	101	10	al.[12	al.[12	PROPN
ecletica-56	101	11	]	]	PUNCT
ecletica-56	101	12	catalayud	catalayud	NOUN
ecletica-56	101	13	et	et	PROPN
ecletica-56	101	14	al	al	PROPN
ecletica-56	101	15	.	.	PUNCT
ecletica-56	102	1	[	[	X
ecletica-56	102	2	13	13	NUM
ecletica-56	102	3	]	]	PUNCT
ecletica-56	102	4	.	.	PUNCT
ecletica-56	103	1	and	and	CCONJ
ecletica-56	103	2	sartorι	sartorι	VERB
ecletica-56	103	3	et	et	PROPN
ecletica-56	103	4	al	al	PROPN
ecletica-56	103	5	.	.	PUNCT
ecletica-56	104	1	[	[	X
ecletica-56	104	2	14	14	NUM
ecletica-56	104	3	]	]	SYM
ecletica-56	104	4	.	.	PUNCT
ecletica-56	104	5	spectrophotometric	spectrophotometric	ADJ
ecletica-56	104	6	methods	method	NOUN
ecletica-56	104	7	for	for	ADP
ecletica-56	104	8	the	the	DET
ecletica-56	104	9	determination	determination	NOUN
ecletica-56	104	10	in	in	ADP
ecletica-56	104	11	bulk	bulk	ADJ
ecletica-56	104	12	drug	drug	NOUN
ecletica-56	104	13	and	and	CCONJ
ecletica-56	104	14	in	in	ADP
ecletica-56	104	15	pharmaceutical	pharmaceutical	ADJ
ecletica-56	104	16	preparations	preparation	NOUN
ecletica-56	104	17	have	have	AUX
ecletica-56	104	18	been	be	AUX
ecletica-56	104	19	also	also	ADV
ecletica-56	104	20	reported	report	VERB
ecletica-56	104	21	.	.	PUNCT
ecletica-56	105	1	in	in	ADP
ecletica-56	105	2	the	the	DET
ecletica-56	105	3	ultraviolet	ultraviolet	NOUN
ecletica-56	105	4	region	region	NOUN
ecletica-56	105	5	methods	method	NOUN
ecletica-56	105	6	some	some	PRON
ecletica-56	105	7	are	be	AUX
ecletica-56	105	8	proposed	propose	VERB
ecletica-56	105	9	:	:	PUNCT
ecletica-56	105	10	british	british	ADJ
ecletica-56	105	11	pharmacopoeia	pharmacopoeia	NOUN
ecletica-56	106	1	[	[	X
ecletica-56	106	2	10	10	NUM
ecletica-56	106	3	]	]	PUNCT
ecletica-56	106	4	,	,	PUNCT
ecletica-56	106	5	annapurna	annapurna	PROPN
ecletica-56	106	6	et	et	PROPN
ecletica-56	106	7	al	al	PROPN
ecletica-56	106	8	.	.	PUNCT
ecletica-56	107	1	[	[	X
ecletica-56	107	2	15	15	NUM
ecletica-56	107	3	]	]	X
ecletica-56	107	4	,	,	PUNCT
ecletica-56	107	5	ashour	ashour	NOUN
ecletica-56	107	6	and	and	CCONJ
ecletica-56	107	7	kabbani[16	kabbani[16	PROPN
ecletica-56	107	8	]	]	X
ecletica-56	107	9	.	.	PUNCT
ecletica-56	108	1	in	in	ADP
ecletica-56	108	2	the	the	DET
ecletica-56	108	3	visible	visible	ADJ
ecletica-56	108	4	region	region	NOUN
ecletica-56	108	5	a	a	DET
ecletica-56	108	6	method	method	NOUN
ecletica-56	108	7	was	be	AUX
ecletica-56	108	8	related	relate	VERB
ecletica-56	108	9	by	by	ADP
ecletica-56	108	10	hassan	hassan	PROPN
ecletica-56	108	11	et	et	PROPN
ecletica-56	108	12	al	al	PROPN
ecletica-56	108	13	.	.	PUNCT
ecletica-56	109	1	[	[	X
ecletica-56	109	2	17	17	NUM
ecletica-56	109	3	]	]	PUNCT
ecletica-56	109	4	.	.	PUNCT
ecletica-56	110	1	this	this	DET
ecletica-56	110	2	last	last	ADJ
ecletica-56	110	3	method	method	NOUN
ecletica-56	110	4	was	be	AUX
ecletica-56	110	5	based	base	VERB
ecletica-56	110	6	of	of	ADP
ecletica-56	110	7	the	the	DET
ecletica-56	110	8	colored	colored	ADJ
ecletica-56	110	9	complex	complex	NOUN
ecletica-56	110	10	formed	form	VERB
ecletica-56	110	11	between	between	ADP
ecletica-56	110	12	metformin	metformin	NOUN
ecletica-56	110	13	(	(	PUNCT
ecletica-56	110	14	mf	mf	X
ecletica-56	110	15	)	)	PUNCT
ecletica-56	110	16	and	and	CCONJ
ecletica-56	110	17	copper	copper	NOUN
ecletica-56	110	18	(	(	PUNCT
ecletica-56	110	19	ii	ii	PROPN
ecletica-56	110	20	)	)	PUNCT
ecletica-56	110	21	with	with	ADP
ecletica-56	110	22	posterior	posterior	ADJ
ecletica-56	110	23	dissolution	dissolution	NOUN
ecletica-56	110	24	in	in	ADP
ecletica-56	110	25	an	an	DET
ecletica-56	110	26	organic	organic	ADJ
ecletica-56	110	27	solvent	solvent	NOUN
ecletica-56	110	28	.	.	PUNCT
ecletica-56	111	1	several	several	ADJ
ecletica-56	111	2	liquid	liquid	ADJ
ecletica-56	111	3	chromatographic	chromatographic	ADJ
ecletica-56	111	4	methods	method	NOUN
ecletica-56	111	5	can	can	AUX
ecletica-56	111	6	been	be	AUX
ecletica-56	111	7	found	find	VERB
ecletica-56	111	8	in	in	ADP
ecletica-56	111	9	the	the	DET
ecletica-56	111	10	literature	literature	NOUN
ecletica-56	111	11	[	[	X
ecletica-56	111	12	8	8	NUM
ecletica-56	111	13	-	-	PUNCT
ecletica-56	111	14	10,18	10,18	NUM
ecletica-56	111	15	-	-	PUNCT
ecletica-56	111	16	23	23	NUM
ecletica-56	111	17	]	]	PUNCT
ecletica-56	111	18	.	.	PUNCT
ecletica-56	112	1	chromatographic	chromatographic	ADJ
ecletica-56	112	2	hplc	hplc	NOUN
ecletica-56	112	3	procedures	procedure	NOUN
ecletica-56	112	4	present	present	VERB
ecletica-56	112	5	good	good	ADJ
ecletica-56	112	6	selectivity	selectivity	NOUN
ecletica-56	112	7	due	due	ADP
ecletica-56	112	8	to	to	ADP
ecletica-56	112	9	the	the	DET
ecletica-56	112	10	separation	separation	NOUN
ecletica-56	112	11	in	in	ADP
ecletica-56	112	12	columns	column	NOUN
ecletica-56	112	13	but	but	CCONJ
ecletica-56	112	14	present	present	VERB
ecletica-56	112	15	an	an	DET
ecletica-56	112	16	environmental	environmental	ADJ
ecletica-56	112	17	disadvantage	disadvantage	NOUN
ecletica-56	112	18	that	that	PRON
ecletica-56	112	19	is	be	AUX
ecletica-56	112	20	the	the	DET
ecletica-56	112	21	relatively	relatively	ADV
ecletica-56	112	22	high	high	ADJ
ecletica-56	112	23	volume	volume	NOUN
ecletica-56	112	24	of	of	ADP
ecletica-56	112	25	organic	organic	ADJ
ecletica-56	112	26	solvents	solvent	NOUN
ecletica-56	112	27	used	use	VERB
ecletica-56	112	28	.	.	PUNCT
ecletica-56	113	1	despite	despite	SCONJ
ecletica-56	113	2	this	this	DET
ecletica-56	113	3	fact	fact	NOUN
ecletica-56	113	4	,	,	PUNCT
ecletica-56	113	5	it	it	PRON
ecletica-56	113	6	can	can	AUX
ecletica-56	113	7	be	be	AUX
ecletica-56	113	8	satisfactorily	satisfactorily	ADV
ecletica-56	113	9	used	use	VERB
ecletica-56	113	10	for	for	ADP
ecletica-56	113	11	the	the	DET
ecletica-56	113	12	simultaneous	simultaneous	ADJ
ecletica-56	113	13	analysis	analysis	NOUN
ecletica-56	113	14	of	of	ADP
ecletica-56	113	15	metformin	metformin	NOUN
ecletica-56	113	16	and	and	CCONJ
ecletica-56	113	17	other	other	ADJ
ecletica-56	113	18	drugs	drug	NOUN
ecletica-56	113	19	present	present	ADJ
ecletica-56	113	20	in	in	ADP
ecletica-56	113	21	the	the	DET
ecletica-56	113	22	same	same	ADJ
ecletica-56	113	23	preparations	preparation	NOUN
ecletica-56	113	24	[	[	X
ecletica-56	113	25	18	18	NUM
ecletica-56	113	26	,	,	PUNCT
ecletica-56	113	27	23	23	NUM
ecletica-56	113	28	-	-	SYM
ecletica-56	113	29	33	33	NUM
ecletica-56	113	30	]	]	PUNCT
ecletica-56	113	31	.	.	PUNCT
ecletica-56	114	1	recently	recently	ADV
ecletica-56	114	2	tubino	tubino	VERB
ecletica-56	114	3	et	et	PROPN
ecletica-56	114	4	al	al	PROPN
ecletica-56	114	5	.	.	PROPN
ecletica-56	114	6	related	relate	VERB
ecletica-56	114	7	an	an	DET
ecletica-56	114	8	analytical	analytical	ADJ
ecletica-56	114	9	quantitative	quantitative	ADJ
ecletica-56	114	10	method	method	NOUN
ecletica-56	114	11	for	for	ADP
ecletica-56	114	12	the	the	DET
ecletica-56	114	13	determination	determination	NOUN
ecletica-56	114	14	of	of	ADP
ecletica-56	114	15	metformin	metformin	NOUN
ecletica-56	114	16	in	in	ADP
ecletica-56	114	17	pharmaceutical	pharmaceutical	ADJ
ecletica-56	114	18	preparations	preparation	NOUN
ecletica-56	114	19	and	and	CCONJ
ecletica-56	114	20	in	in	ADP
ecletica-56	114	21	the	the	DET
ecletica-56	114	22	bulk	bulk	ADJ
ecletica-56	114	23	drug	drug	NOUN
ecletica-56	114	24	using	use	VERB
ecletica-56	114	25	diffuse	diffuse	NOUN
ecletica-56	114	26	ultraviolet	ultraviolet	ADJ
ecletica-56	114	27	-	-	PUNCT
ecletica-56	114	28	visible	visible	ADJ
ecletica-56	114	29	reflectance	reflectance	NOUN
ecletica-56	115	1	[	[	X
ecletica-56	115	2	34	34	NUM
ecletica-56	115	3	]	]	PUNCT
ecletica-56	115	4	.	.	PUNCT
ecletica-56	116	1	despite	despite	SCONJ
ecletica-56	116	2	the	the	DET
ecletica-56	116	3	reporting	reporting	NOUN
ecletica-56	116	4	of	of	ADP
ecletica-56	116	5	a	a	DET
ecletica-56	116	6	number	number	NOUN
ecletica-56	116	7	of	of	ADP
ecletica-56	116	8	methods	method	NOUN
ecletica-56	116	9	for	for	ADP
ecletica-56	116	10	the	the	DET
ecletica-56	116	11	analysis	analysis	NOUN
ecletica-56	116	12	of	of	ADP
ecletica-56	116	13	metformin	metformin	NOUN
ecletica-56	116	14	,	,	PUNCT
ecletica-56	116	15	a	a	DET
ecletica-56	116	16	deficiency	deficiency	NOUN
ecletica-56	116	17	is	be	AUX
ecletica-56	116	18	observed	observe	VERB
ecletica-56	116	19	with	with	ADP
ecletica-56	116	20	respect	respect	NOUN
ecletica-56	116	21	to	to	ADP
ecletica-56	116	22	absolute	absolute	ADJ
ecletica-56	116	23	methods	method	NOUN
ecletica-56	116	24	,	,	PUNCT
ecletica-56	116	25	i.e.	i.e.	X
ecletica-56	116	26	,	,	PUNCT
ecletica-56	116	27	that	that	PRON
ecletica-56	116	28	do	do	AUX
ecletica-56	116	29	not	not	PART
ecletica-56	116	30	require	require	VERB
ecletica-56	116	31	calibration	calibration	NOUN
ecletica-56	116	32	curves	curve	NOUN
ecletica-56	116	33	.	.	PUNCT
ecletica-56	117	1	only	only	ADV
ecletica-56	117	2	three	three	NUM
ecletica-56	117	3	volumetric	volumetric	NOUN
ecletica-56	117	4	[	[	X
ecletica-56	117	5	1214	1214	NUM
ecletica-56	117	6	]	]	PUNCT
ecletica-56	117	7	are	be	AUX
ecletica-56	117	8	reported	report	VERB
ecletica-56	117	9	and	and	CCONJ
ecletica-56	117	10	no	no	DET
ecletica-56	117	11	one	one	NOUN
ecletica-56	117	12	for	for	ADP
ecletica-56	117	13	gravimetric	gravimetric	ADJ
ecletica-56	117	14	was	be	AUX
ecletica-56	117	15	found	find	VERB
ecletica-56	117	16	.	.	PUNCT
ecletica-56	118	1	despite	despite	SCONJ
ecletica-56	118	2	their	their	PRON
ecletica-56	118	3	absolute	absolute	ADJ
ecletica-56	118	4	analytical	analytical	ADJ
ecletica-56	118	5	characteristic	characteristic	ADJ
ecletica-56	118	6	classical	classical	ADJ
ecletica-56	118	7	gravimetric	gravimetric	ADJ
ecletica-56	118	8	methods	method	NOUN
ecletica-56	118	9	are	be	AUX
ecletica-56	118	10	usually	usually	ADV
ecletica-56	118	11	very	very	ADV
ecletica-56	118	12	slow	slow	ADJ
ecletica-56	118	13	.	.	PUNCT
ecletica-56	119	1	however	however	ADV
ecletica-56	119	2	,	,	PUNCT
ecletica-56	119	3	the	the	DET
ecletica-56	119	4	developing	developing	NOUN
ecletica-56	119	5	of	of	ADP
ecletica-56	119	6	the	the	DET
ecletica-56	119	7	weighing	weighing	NOUN
ecletica-56	119	8	techniques	technique	NOUN
ecletica-56	119	9	that	that	PRON
ecletica-56	119	10	resulted	result	VERB
ecletica-56	119	11	in	in	ADP
ecletica-56	119	12	better	well	ADJ
ecletica-56	119	13	and	and	CCONJ
ecletica-56	119	14	faster	fast	ADV
ecletica-56	119	15	to	to	PART
ecletica-56	119	16	use	use	VERB
ecletica-56	119	17	balances	balance	NOUN
ecletica-56	119	18	,	,	PUNCT
ecletica-56	119	19	relatively	relatively	ADV
ecletica-56	119	20	fast	fast	ADJ
ecletica-56	119	21	gravimetric	gravimetric	ADJ
ecletica-56	119	22	procedures	procedure	NOUN
ecletica-56	119	23	can	can	AUX
ecletica-56	119	24	be	be	AUX
ecletica-56	119	25	developed	develop	VERB
ecletica-56	119	26	[	[	X
ecletica-56	119	27	35	35	NUM
ecletica-56	119	28	]	]	PUNCT
ecletica-56	119	29	.	.	PUNCT
ecletica-56	120	1	the	the	DET
ecletica-56	120	2	aim	aim	NOUN
ecletica-56	120	3	of	of	ADP
ecletica-56	120	4	the	the	DET
ecletica-56	120	5	present	present	ADJ
ecletica-56	120	6	work	work	NOUN
ecletica-56	120	7	was	be	AUX
ecletica-56	120	8	to	to	PART
ecletica-56	120	9	develop	develop	VERB
ecletica-56	120	10	a	a	DET
ecletica-56	120	11	reliable	reliable	ADJ
ecletica-56	120	12	,	,	PUNCT
ecletica-56	120	13	simple	simple	ADJ
ecletica-56	120	14	and	and	CCONJ
ecletica-56	120	15	relatively	relatively	ADV
ecletica-56	120	16	fast	fast	ADJ
ecletica-56	120	17	method	method	NOUN
ecletica-56	120	18	for	for	ADP
ecletica-56	120	19	the	the	DET
ecletica-56	120	20	determination	determination	NOUN
ecletica-56	120	21	of	of	ADP
ecletica-56	120	22	metformin	metformin	NOUN
ecletica-56	120	23	in	in	ADP
ecletica-56	120	24	bulk	bulk	ADJ
ecletica-56	120	25	drugs	drug	NOUN
ecletica-56	120	26	and	and	CCONJ
ecletica-56	120	27	in	in	ADP
ecletica-56	120	28	pharmaceutical	pharmaceutical	ADJ
ecletica-56	120	29	preparations	preparation	NOUN
ecletica-56	120	30	.	.	PUNCT
ecletica-56	121	1	experimental	experimental	ADJ
ecletica-56	121	2	details	detail	NOUN
ecletica-56	121	3	apparatus	apparatus	NOUN
ecletica-56	121	4	hplc	hplc	NOUN
ecletica-56	121	5	:	:	PUNCT
ecletica-56	121	6	shimadzu	shimadzu	ADJ
ecletica-56	121	7	prominence	prominence	NOUN
ecletica-56	121	8	diode	diode	NOUN
ecletica-56	121	9	array	array	NOUN
ecletica-56	121	10	sppm20	sppm20	NOUN
ecletica-56	121	11	;	;	PUNCT
ecletica-56	121	12	micro	micro	ADJ
ecletica-56	121	13	-	-	PROPN
ecletica-56	121	14	bondapac	bondapac	ADJ
ecletica-56	121	15	column	column	NOUN
ecletica-56	121	16	c18	c18	NOUN
ecletica-56	121	17	,	,	PUNCT
ecletica-56	121	18	length	length	NOUN
ecletica-56	121	19	300	300	NUM
ecletica-56	121	20	mm	mm	NOUN
ecletica-56	121	21	,	,	PUNCT
ecletica-56	121	22	i.d	i.d	PROPN
ecletica-56	121	23	.	.	PROPN
ecletica-56	121	24	3.0	3.0	NUM
ecletica-56	121	25	mm	mm	NOUN
ecletica-56	121	26	,	,	PUNCT
ecletica-56	121	27	particle	particle	NOUN
ecletica-56	121	28	size	size	NOUN
ecletica-56	121	29	10	10	NUM
ecletica-56	121	30	m	m	PROPN
ecletica-56	121	31	.	.	PUNCT
ecletica-56	122	1	injection	injection	NOUN
ecletica-56	122	2	volume	volume	NOUN
ecletica-56	122	3	20	20	NUM
ecletica-56	122	4	l	l	PROPN
ecletica-56	122	5	.	.	PUNCT
ecletica-56	123	1	phmeter	phmeter	NOUN
ecletica-56	123	2	:	:	PUNCT
ecletica-56	124	1	analyser	analyser	NOUN
ecletica-56	124	2	,	,	PUNCT
ecletica-56	124	3	model	model	NOUN
ecletica-56	124	4	ph	ph	NOUN
ecletica-56	124	5	300	300	NUM
ecletica-56	124	6	,	,	PUNCT
ecletica-56	124	7	with	with	ADP
ecletica-56	124	8	a	a	DET
ecletica-56	124	9	glass	glass	NOUN
ecletica-56	124	10	combined	combine	VERB
ecletica-56	124	11	ag	ag	PROPN
ecletica-56	124	12	/	/	SYM
ecletica-56	124	13	agcl	agcl	NOUN
ecletica-56	124	14	electrode	electrode	NOUN
ecletica-56	124	15	;	;	PUNCT
ecletica-56	124	16	internal	internal	ADJ
ecletica-56	124	17	solution	solution	NOUN
ecletica-56	124	18	kcl	kcl	PROPN
ecletica-56	124	19	3.0	3.0	NUM
ecletica-56	124	20	mol	mol	ADP
ecletica-56	124	21	l	l	NOUN
ecletica-56	124	22	-1	-1	PUNCT
ecletica-56	124	23	.	.	PUNCT
ecletica-56	125	1	reagents	reagent	NOUN
ecletica-56	125	2	all	all	DET
ecletica-56	125	3	the	the	DET
ecletica-56	125	4	employed	employ	VERB
ecletica-56	125	5	reagents	reagent	NOUN
ecletica-56	125	6	were	be	AUX
ecletica-56	125	7	of	of	ADP
ecletica-56	125	8	analytical	analytical	ADJ
ecletica-56	125	9	grade	grade	NOUN
ecletica-56	125	10	,	,	PUNCT
ecletica-56	125	11	excepting	except	VERB
ecletica-56	125	12	the	the	DET
ecletica-56	125	13	metformin	metformin	NOUN
ecletica-56	125	14	hydrochloride	hydrochloride	NOUN
ecletica-56	125	15	that	that	PRON
ecletica-56	125	16	was	be	AUX
ecletica-56	125	17	a	a	DET
ecletica-56	125	18	pharmaceutical	pharmaceutical	ADJ
ecletica-56	125	19	grade	grade	NOUN
ecletica-56	125	20	98.5	98.5	NUM
ecletica-56	125	21	%	%	NOUN
ecletica-56	125	22	,	,	PUNCT
ecletica-56	125	23	certified	certified	ADJ
ecletica-56	125	24	product	product	NOUN
ecletica-56	125	25	.	.	PUNCT
ecletica-56	126	1	the	the	DET
ecletica-56	126	2	pharmaceutical	pharmaceutical	ADJ
ecletica-56	126	3	preparations	preparation	NOUN
ecletica-56	126	4	were	be	AUX
ecletica-56	126	5	purchased	purchase	VERB
ecletica-56	126	6	in	in	ADP
ecletica-56	126	7	drugstores	drugstore	NOUN
ecletica-56	126	8	of	of	ADP
ecletica-56	126	9	the	the	DET
ecletica-56	126	10	region	region	NOUN
ecletica-56	126	11	.	.	PUNCT
ecletica-56	127	1	eclética	eclética	PROPN
ecletica-56	127	2	química	química	PROPN
ecletica-56	127	3	,	,	PUNCT
ecletica-56	127	4	vol	vol	NOUN
ecletica-56	127	5	.	.	PROPN
ecletica-56	127	6	40	40	NUM
ecletica-56	127	7	,	,	PUNCT
ecletica-56	127	8	62	62	NUM
ecletica-56	127	9	-	-	SYM
ecletica-56	127	10	70	70	NUM
ecletica-56	127	11	,	,	PUNCT
ecletica-56	127	12	2015	2015	NUM
ecletica-56	127	13	.	.	PUNCT
ecletica-56	128	1	64	64	NUM
ecletica-56	128	2	64	64	NUM
ecletica-56	128	3	solutions	solution	NOUN
ecletica-56	128	4	standard	standard	ADJ
ecletica-56	128	5	solution	solution	NOUN
ecletica-56	128	6	of	of	ADP
ecletica-56	128	7	metformin	metformin	NOUN
ecletica-56	128	8	hydrochloride	hydrochloride	NOUN
ecletica-56	128	9	:	:	PUNCT
ecletica-56	128	10	prepared	prepare	VERB
ecletica-56	128	11	in	in	ADP
ecletica-56	128	12	calibrated	calibrate	VERB
ecletica-56	128	13	50	50	NUM
ecletica-56	128	14	ml	ml	NOUN
ecletica-56	128	15	volumetric	volumetric	ADJ
ecletica-56	128	16	flask	flask	NOUN
ecletica-56	128	17	;	;	PUNCT
ecletica-56	128	18	about	about	ADV
ecletica-56	128	19	7.5	7.5	NUM
ecletica-56	128	20	grams	gram	NOUN
ecletica-56	128	21	(	(	PUNCT
ecletica-56	128	22	weighed	weigh	VERB
ecletica-56	128	23	to	to	ADP
ecletica-56	128	24	0.1	0.1	NUM
ecletica-56	128	25	mg	mg	NOUN
ecletica-56	128	26	)	)	PUNCT
ecletica-56	128	27	of	of	ADP
ecletica-56	128	28	the	the	DET
ecletica-56	128	29	drug	drug	NOUN
ecletica-56	128	30	(	(	PUNCT
ecletica-56	128	31	98.5	98.5	NUM
ecletica-56	128	32	%	%	NOUN
ecletica-56	128	33	certified	certify	VERB
ecletica-56	128	34	metformin	metformin	NOUN
ecletica-56	128	35	hydrochloride	hydrochloride	NOUN
ecletica-56	128	36	)	)	PUNCT
ecletica-56	128	37	was	be	AUX
ecletica-56	128	38	dissolved	dissolve	VERB
ecletica-56	128	39	in	in	ADP
ecletica-56	128	40	milli	milli	ADJ
ecletica-56	128	41	q	q	ADJ
ecletica-56	128	42	pure	pure	ADJ
ecletica-56	128	43	class	class	NOUN
ecletica-56	128	44	water	water	NOUN
ecletica-56	128	45	.	.	PUNCT
ecletica-56	129	1	nickel	nickel	NOUN
ecletica-56	129	2	chloride	chloride	PROPN
ecletica-56	129	3	1	1	NUM
ecletica-56	129	4	mol	mol	ADP
ecletica-56	129	5	l	l	NOUN
ecletica-56	129	6	-1	-1	NOUN
ecletica-56	129	7	solution	solution	NOUN
ecletica-56	129	8	:	:	PUNCT
ecletica-56	129	9	11.9	11.9	NUM
ecletica-56	129	10	g	g	NOUN
ecletica-56	129	11	of	of	ADP
ecletica-56	129	12	nicl2·6h2o	nicl2·6h2o	NOUN
ecletica-56	129	13	were	be	AUX
ecletica-56	129	14	dissolved	dissolve	VERB
ecletica-56	129	15	with	with	ADP
ecletica-56	129	16	milli	milli	ADJ
ecletica-56	129	17	q	q	ADJ
ecletica-56	129	18	pure	pure	ADJ
ecletica-56	129	19	grade	grade	NOUN
ecletica-56	129	20	water	water	NOUN
ecletica-56	129	21	in	in	ADP
ecletica-56	129	22	a	a	DET
ecletica-56	129	23	50	50	NUM
ecletica-56	129	24	ml	ml	NOUN
ecletica-56	129	25	volumetric	volumetric	ADJ
ecletica-56	129	26	flask	flask	NOUN
ecletica-56	129	27	.	.	PUNCT
ecletica-56	130	1	naoh	naoh	NOUN
ecletica-56	130	2	2	2	NUM
ecletica-56	130	3	mol	mol	ADP
ecletica-56	130	4	l	l	NOUN
ecletica-56	130	5	-1	-1	NOUN
ecletica-56	130	6	solution	solution	NOUN
ecletica-56	130	7	:	:	PUNCT
ecletica-56	130	8	4.0	4.0	NUM
ecletica-56	130	9	g	g	NOUN
ecletica-56	130	10	of	of	ADP
ecletica-56	130	11	naoh	naoh	NOUN
ecletica-56	130	12	were	be	AUX
ecletica-56	130	13	dissolved	dissolve	VERB
ecletica-56	130	14	in	in	ADP
ecletica-56	130	15	milli	milli	ADJ
ecletica-56	130	16	q	q	ADJ
ecletica-56	130	17	pure	pure	ADJ
ecletica-56	130	18	grade	grade	NOUN
ecletica-56	130	19	water	water	NOUN
ecletica-56	130	20	in	in	ADP
ecletica-56	130	21	a	a	DET
ecletica-56	130	22	50	50	NUM
ecletica-56	130	23	ml	ml	NOUN
ecletica-56	130	24	volumetric	volumetric	ADJ
ecletica-56	130	25	flask	flask	NOUN
ecletica-56	130	26	.	.	PUNCT
ecletica-56	131	1	hclo4	hclo4	NOUN
ecletica-56	131	2	0.1	0.1	NUM
ecletica-56	131	3	mol	mol	ADP
ecletica-56	131	4	l	l	NOUN
ecletica-56	131	5	-1	-1	NOUN
ecletica-56	131	6	in	in	ADP
ecletica-56	131	7	glacial	glacial	ADJ
ecletica-56	131	8	acetic	acetic	ADJ
ecletica-56	131	9	acid	acid	NOUN
ecletica-56	132	1	[	[	X
ecletica-56	132	2	11	11	NUM
ecletica-56	132	3	]	]	SYM
ecletica-56	132	4	:	:	PUNCT
ecletica-56	132	5	8.5	8.5	NUM
ecletica-56	132	6	ml	ml	NOUN
ecletica-56	132	7	of	of	ADP
ecletica-56	132	8	perchloric	perchloric	ADJ
ecletica-56	132	9	acid	acid	NOUN
ecletica-56	132	10	were	be	AUX
ecletica-56	132	11	dissolved	dissolve	VERB
ecletica-56	132	12	in	in	ADP
ecletica-56	132	13	500	500	NUM
ecletica-56	132	14	ml	ml	NOUN
ecletica-56	132	15	of	of	ADP
ecletica-56	132	16	glacial	glacial	ADJ
ecletica-56	132	17	acetic	acetic	ADJ
ecletica-56	132	18	acid	acid	NOUN
ecletica-56	132	19	;	;	PUNCT
ecletica-56	132	20	21	21	NUM
ecletica-56	132	21	ml	ml	NOUN
ecletica-56	132	22	of	of	ADP
ecletica-56	132	23	acetic	acetic	ADJ
ecletica-56	132	24	anhydride	anhydride	NOUN
ecletica-56	132	25	were	be	AUX
ecletica-56	132	26	added	add	VERB
ecletica-56	132	27	;	;	PUNCT
ecletica-56	132	28	the	the	DET
ecletica-56	132	29	volume	volume	NOUN
ecletica-56	132	30	was	be	AUX
ecletica-56	132	31	completed	complete	VERB
ecletica-56	132	32	to	to	ADP
ecletica-56	132	33	1000	1000	NUM
ecletica-56	132	34	ml	ml	NOUN
ecletica-56	132	35	with	with	ADP
ecletica-56	132	36	glacial	glacial	ADJ
ecletica-56	132	37	acetic	acetic	ADJ
ecletica-56	132	38	acid	acid	NOUN
ecletica-56	132	39	.	.	PUNCT
ecletica-56	133	1	the	the	DET
ecletica-56	133	2	solution	solution	NOUN
ecletica-56	133	3	was	be	AUX
ecletica-56	133	4	standardized	standardize	VERB
ecletica-56	133	5	with	with	ADP
ecletica-56	133	6	potassium	potassium	NOUN
ecletica-56	133	7	biphthalate	biphthalate	NOUN
ecletica-56	133	8	.	.	PUNCT
ecletica-56	134	1	standard	standard	NOUN
ecletica-56	134	2	(	(	PUNCT
ecletica-56	134	3	nh4)h2po4	nh4)h2po4	PROPN
ecletica-56	134	4	ph	ph	VERB
ecletica-56	134	5	5.00	5.00	NUM
ecletica-56	134	6	buffer	buffer	NOUN
ecletica-56	134	7	solution	solution	NOUN
ecletica-56	134	8	:	:	PUNCT
ecletica-56	134	9	5.0	5.0	NUM
ecletica-56	134	10	g	g	NOUN
ecletica-56	134	11	of	of	ADP
ecletica-56	134	12	the	the	DET
ecletica-56	134	13	salt	salt	NOUN
ecletica-56	134	14	were	be	AUX
ecletica-56	134	15	dissolved	dissolve	VERB
ecletica-56	134	16	in	in	ADP
ecletica-56	134	17	500	500	NUM
ecletica-56	134	18	ml	ml	NOUN
ecletica-56	134	19	of	of	ADP
ecletica-56	134	20	pure	pure	ADJ
ecletica-56	134	21	water	water	NOUN
ecletica-56	134	22	.	.	PUNCT
ecletica-56	135	1	the	the	DET
ecletica-56	135	2	ph	ph	PROPN
ecletica-56	135	3	was	be	AUX
ecletica-56	135	4	adjusted	adjust	VERB
ecletica-56	135	5	with	with	ADP
ecletica-56	135	6	naoh	naoh	NOUN
ecletica-56	135	7	0.2	0.2	NUM
ecletica-56	135	8	mol	mol	ADP
ecletica-56	135	9	l	l	NOUN
ecletica-56	135	10	-1	-1	PUNCT
ecletica-56	135	11	,	,	PUNCT
ecletica-56	135	12	prepared	prepare	VERB
ecletica-56	135	13	by	by	ADP
ecletica-56	135	14	dilution	dilution	NOUN
ecletica-56	135	15	from	from	ADP
ecletica-56	135	16	that	that	PRON
ecletica-56	135	17	of	of	ADP
ecletica-56	135	18	2.0	2.0	NUM
ecletica-56	135	19	mol	mol	ADP
ecletica-56	135	20	l	l	NOUN
ecletica-56	135	21	-1	-1	PUNCT
ecletica-56	135	22	,	,	PUNCT
ecletica-56	135	23	to	to	ADP
ecletica-56	135	24	ph	ph	NOUN
ecletica-56	135	25	=	=	PUNCT
ecletica-56	136	1	5.00	5.00	NUM
ecletica-56	136	2			PROPN
ecletica-56	136	3	0.05	0.05	NUM
ecletica-56	136	4	.	.	PUNCT
ecletica-56	136	5	mobile	mobile	ADJ
ecletica-56	136	6	phase	phase	NOUN
ecletica-56	136	7	,	,	PUNCT
ecletica-56	136	8	hplc	hplc	NOUN
ecletica-56	136	9	:	:	PUNCT
ecletica-56	136	10	500	500	NUM
ecletica-56	136	11	ml	ml	NOUN
ecletica-56	136	12	of	of	ADP
ecletica-56	136	13	methanol	methanol	NOUN
ecletica-56	136	14	and	and	CCONJ
ecletica-56	136	15	500	500	NUM
ecletica-56	136	16	ml	ml	NOUN
ecletica-56	136	17	of	of	ADP
ecletica-56	136	18	the	the	DET
ecletica-56	136	19	(	(	PUNCT
ecletica-56	136	20	nh4)h2po4	nh4)h2po4	PROPN
ecletica-56	136	21	buffer	buffer	NOUN
ecletica-56	136	22	[	[	X
ecletica-56	136	23	28	28	NUM
ecletica-56	136	24	]	]	PUNCT
ecletica-56	136	25	.	.	PUNCT
ecletica-56	137	1	standard	standard	ADJ
ecletica-56	137	2	solutions	solution	NOUN
ecletica-56	137	3	for	for	ADP
ecletica-56	137	4	the	the	DET
ecletica-56	137	5	calibration	calibration	NOUN
ecletica-56	137	6	curve	curve	NOUN
ecletica-56	137	7	,	,	PUNCT
ecletica-56	137	8	hplc	hplc	NOUN
ecletica-56	137	9	:	:	PUNCT
ecletica-56	137	10	507.6	507.6	NUM
ecletica-56	137	11	mg	mg	NOUN
ecletica-56	137	12	of	of	ADP
ecletica-56	137	13	the	the	DET
ecletica-56	137	14	drug	drug	NOUN
ecletica-56	137	15	(	(	PUNCT
ecletica-56	137	16	containing	contain	VERB
ecletica-56	137	17	500.0	500.0	NUM
ecletica-56	137	18	mg	mg	NOUN
ecletica-56	137	19	of	of	ADP
ecletica-56	137	20	metformin	metformin	NOUN
ecletica-56	137	21	hydrochloride	hydrochloride	NOUN
ecletica-56	137	22	)	)	PUNCT
ecletica-56	137	23	was	be	AUX
ecletica-56	137	24	exactly	exactly	ADV
ecletica-56	137	25	weighed	weigh	VERB
ecletica-56	137	26	and	and	CCONJ
ecletica-56	137	27	transferred	transfer	VERB
ecletica-56	137	28	to	to	ADP
ecletica-56	137	29	a	a	DET
ecletica-56	137	30	100.0	100.0	NUM
ecletica-56	137	31	ml	ml	NOUN
ecletica-56	137	32	volumetric	volumetric	ADJ
ecletica-56	137	33	flask	flask	NOUN
ecletica-56	137	34	and	and	CCONJ
ecletica-56	137	35	dissolved	dissolve	VERB
ecletica-56	137	36	with	with	ADP
ecletica-56	137	37	50.0	50.0	NUM
ecletica-56	137	38	ml	ml	NOUN
ecletica-56	137	39	of	of	ADP
ecletica-56	137	40	methanol	methanol	NOUN
ecletica-56	137	41	.	.	PUNCT
ecletica-56	138	1	the	the	DET
ecletica-56	138	2	volume	volume	NOUN
ecletica-56	138	3	was	be	AUX
ecletica-56	138	4	completed	complete	VERB
ecletica-56	138	5	with	with	ADP
ecletica-56	138	6	the	the	DET
ecletica-56	138	7	ph	ph	ADJ
ecletica-56	138	8	5.00	5.00	NUM
ecletica-56	138	9	buffer	buffer	NOUN
ecletica-56	138	10	solution	solution	NOUN
ecletica-56	138	11	.	.	PUNCT
ecletica-56	139	1	from	from	ADP
ecletica-56	139	2	this	this	DET
ecletica-56	139	3	5000	5000	NUM
ecletica-56	139	4	ppm	ppm	NOUN
ecletica-56	139	5	solution	solution	NOUN
ecletica-56	139	6	8.00	8.00	NUM
ecletica-56	139	7	ml	ml	NOUN
ecletica-56	139	8	were	be	AUX
ecletica-56	139	9	taken	take	VERB
ecletica-56	139	10	and	and	CCONJ
ecletica-56	139	11	transferred	transfer	VERB
ecletica-56	139	12	to	to	ADP
ecletica-56	139	13	a	a	DET
ecletica-56	139	14	200.0	200.0	NUM
ecletica-56	139	15	ml	ml	NOUN
ecletica-56	139	16	volumetric	volumetric	NOUN
ecletica-56	139	17	balloon	balloon	NOUN
ecletica-56	139	18	.	.	PUNCT
ecletica-56	140	1	the	the	DET
ecletica-56	140	2	volume	volume	NOUN
ecletica-56	140	3	was	be	AUX
ecletica-56	140	4	completed	complete	VERB
ecletica-56	140	5	with	with	ADP
ecletica-56	140	6	the	the	DET
ecletica-56	140	7	mobile	mobile	ADJ
ecletica-56	140	8	phase	phase	NOUN
ecletica-56	140	9	above	above	ADP
ecletica-56	140	10	described	describe	VERB
ecletica-56	140	11	.	.	PUNCT
ecletica-56	141	1	from	from	ADP
ecletica-56	141	2	this	this	DET
ecletica-56	141	3	200.0	200.0	NUM
ecletica-56	141	4	ppm	ppm	NOUN
ecletica-56	141	5	stock	stock	NOUN
ecletica-56	141	6	solution	solution	NOUN
ecletica-56	141	7	120.0	120.0	NUM
ecletica-56	141	8	,	,	PUNCT
ecletica-56	141	9	130.0	130.0	NUM
ecletica-56	141	10	,	,	PUNCT
ecletica-56	141	11	140.0	140.0	NUM
ecletica-56	141	12	,	,	PUNCT
ecletica-56	141	13	150.0	150.0	NUM
ecletica-56	141	14	,	,	PUNCT
ecletica-56	141	15	160.0	160.0	NUM
ecletica-56	141	16	,	,	PUNCT
ecletica-56	141	17	and	and	CCONJ
ecletica-56	141	18	170.0	170.0	NUM
ecletica-56	141	19	ppm	ppm	NOUN
ecletica-56	141	20	concentrations	concentration	NOUN
ecletica-56	141	21	were	be	AUX
ecletica-56	141	22	obtained	obtain	VERB
ecletica-56	141	23	through	through	ADP
ecletica-56	141	24	adequate	adequate	ADJ
ecletica-56	141	25	dilutions	dilution	NOUN
ecletica-56	141	26	.	.	PUNCT
ecletica-56	142	1	samples	sample	NOUN
ecletica-56	142	2	treatment	treatment	NOUN
ecletica-56	142	3	proposed	propose	VERB
ecletica-56	142	4	method	method	NOUN
ecletica-56	142	5	20	20	NUM
ecletica-56	142	6	tablets	tablet	NOUN
ecletica-56	142	7	were	be	AUX
ecletica-56	142	8	accurately	accurately	ADV
ecletica-56	142	9	weighed	weigh	VERB
ecletica-56	142	10	in	in	ADP
ecletica-56	142	11	an	an	DET
ecletica-56	142	12	analytical	analytical	ADJ
ecletica-56	142	13	balance	balance	NOUN
ecletica-56	142	14	to	to	ADP
ecletica-56	142	15	0.1	0.1	NUM
ecletica-56	142	16	mg	mg	NOUN
ecletica-56	142	17	.	.	PUNCT
ecletica-56	143	1	from	from	ADP
ecletica-56	143	2	the	the	DET
ecletica-56	143	3	total	total	ADJ
ecletica-56	143	4	mass	mass	NOUN
ecletica-56	143	5	the	the	DET
ecletica-56	143	6	mean	mean	ADJ
ecletica-56	143	7	weight	weight	NOUN
ecletica-56	143	8	of	of	ADP
ecletica-56	143	9	a	a	DET
ecletica-56	143	10	tablet	tablet	NOUN
ecletica-56	143	11	was	be	AUX
ecletica-56	143	12	calculated	calculate	VERB
ecletica-56	143	13	.	.	PUNCT
ecletica-56	144	1	an	an	DET
ecletica-56	144	2	aliquot	aliquot	NOUN
ecletica-56	144	3	of	of	ADP
ecletica-56	144	4	about	about	ADP
ecletica-56	144	5	1.0	1.0	NUM
ecletica-56	144	6	g	g	NOUN
ecletica-56	144	7	(	(	PUNCT
ecletica-56	144	8	about	about	ADP
ecletica-56	144	9	800	800	NUM
ecletica-56	144	10	mg	mg	NOUN
ecletica-56	144	11	of	of	ADP
ecletica-56	144	12	metformin	metformin	NOUN
ecletica-56	144	13	hydrochloride	hydrochloride	NOUN
ecletica-56	144	14	)	)	PUNCT
ecletica-56	144	15	with	with	ADP
ecletica-56	144	16	accuracy	accuracy	NOUN
ecletica-56	144	17	of	of	ADP
ecletica-56	144	18	0.1	0.1	NUM
ecletica-56	144	19	mg	mg	NOUN
ecletica-56	144	20	was	be	AUX
ecletica-56	144	21	weighed	weigh	VERB
ecletica-56	144	22	into	into	ADP
ecletica-56	144	23	an	an	DET
ecletica-56	144	24	essay	essay	ADJ
ecletica-56	144	25	tube	tube	NOUN
ecletica-56	144	26	.	.	PUNCT
ecletica-56	145	1	2.0	2.0	NUM
ecletica-56	145	2	ml	ml	NOUN
ecletica-56	145	3	of	of	ADP
ecletica-56	145	4	water	water	NOUN
ecletica-56	145	5	were	be	AUX
ecletica-56	145	6	added	add	VERB
ecletica-56	145	7	following	follow	VERB
ecletica-56	145	8	stirring	stir	VERB
ecletica-56	145	9	to	to	PART
ecletica-56	145	10	dissolve	dissolve	VERB
ecletica-56	145	11	the	the	DET
ecletica-56	145	12	drug	drug	NOUN
ecletica-56	145	13	and	and	CCONJ
ecletica-56	145	14	centrifugation	centrifugation	NOUN
ecletica-56	145	15	during	during	ADP
ecletica-56	145	16	5	5	NUM
ecletica-56	145	17	minutes	minute	NOUN
ecletica-56	145	18	at	at	ADP
ecletica-56	145	19	4500	4500	NUM
ecletica-56	145	20	rpm	rpm	NOUN
ecletica-56	145	21	to	to	PART
ecletica-56	145	22	separate	separate	VERB
ecletica-56	145	23	no	no	DET
ecletica-56	145	24	soluble	soluble	ADJ
ecletica-56	145	25	excipients	excipient	NOUN
ecletica-56	145	26	.	.	PUNCT
ecletica-56	146	1	the	the	DET
ecletica-56	146	2	supernatant	supernatant	NOUN
ecletica-56	146	3	was	be	AUX
ecletica-56	146	4	carefully	carefully	ADV
ecletica-56	146	5	transferred	transfer	VERB
ecletica-56	146	6	to	to	ADP
ecletica-56	146	7	a	a	DET
ecletica-56	146	8	10.0	10.0	NUM
ecletica-56	146	9	ml	ml	NOUN
ecletica-56	146	10	volumetric	volumetric	ADJ
ecletica-56	146	11	flask	flask	NOUN
ecletica-56	146	12	.	.	PUNCT
ecletica-56	147	1	2.0	2.0	NUM
ecletica-56	147	2	ml	ml	ADP
ecletica-56	147	3	more	more	ADJ
ecletica-56	147	4	were	be	AUX
ecletica-56	147	5	added	add	VERB
ecletica-56	147	6	to	to	ADP
ecletica-56	147	7	the	the	DET
ecletica-56	147	8	residue	residue	NOUN
ecletica-56	147	9	into	into	ADP
ecletica-56	147	10	the	the	DET
ecletica-56	147	11	tube	tube	NOUN
ecletica-56	147	12	and	and	CCONJ
ecletica-56	147	13	the	the	DET
ecletica-56	147	14	process	process	NOUN
ecletica-56	147	15	was	be	AUX
ecletica-56	147	16	repeated	repeat	VERB
ecletica-56	147	17	.	.	PUNCT
ecletica-56	148	1	three	three	NUM
ecletica-56	148	2	extraction	extraction	NOUN
ecletica-56	148	3	were	be	AUX
ecletica-56	148	4	performed	perform	VERB
ecletica-56	148	5	and	and	CCONJ
ecletica-56	148	6	always	always	ADV
ecletica-56	148	7	the	the	DET
ecletica-56	148	8	supernatant	supernatant	NOUN
ecletica-56	148	9	was	be	AUX
ecletica-56	148	10	introduced	introduce	VERB
ecletica-56	148	11	into	into	ADP
ecletica-56	148	12	the	the	DET
ecletica-56	148	13	10.0	10.0	NUM
ecletica-56	148	14	ml	ml	NOUN
ecletica-56	148	15	balloon	balloon	NOUN
ecletica-56	148	16	.	.	PUNCT
ecletica-56	149	1	the	the	DET
ecletica-56	149	2	volume	volume	NOUN
ecletica-56	149	3	was	be	AUX
ecletica-56	149	4	completed	complete	VERB
ecletica-56	149	5	to	to	ADP
ecletica-56	149	6	the	the	DET
ecletica-56	149	7	mark	mark	NOUN
ecletica-56	149	8	with	with	ADP
ecletica-56	149	9	water	water	NOUN
ecletica-56	149	10	.	.	PUNCT
ecletica-56	150	1	hplc	hplc	NOUN
ecletica-56	150	2	method	method	NOUN
ecletica-56	150	3	[	[	X
ecletica-56	150	4	28	28	NUM
ecletica-56	150	5	]	]	SYM
ecletica-56	150	6	20	20	NUM
ecletica-56	150	7	tablets	tablet	NOUN
ecletica-56	150	8	were	be	AUX
ecletica-56	150	9	accurately	accurately	ADV
ecletica-56	150	10	weighed	weigh	VERB
ecletica-56	150	11	in	in	ADP
ecletica-56	150	12	an	an	DET
ecletica-56	150	13	analytical	analytical	ADJ
ecletica-56	150	14	balance	balance	NOUN
ecletica-56	150	15	to	to	ADP
ecletica-56	150	16	0.1	0.1	NUM
ecletica-56	150	17	mg	mg	NOUN
ecletica-56	150	18	and	and	CCONJ
ecletica-56	150	19	carefully	carefully	ADV
ecletica-56	150	20	crushed	crush	VERB
ecletica-56	150	21	in	in	ADP
ecletica-56	150	22	a	a	DET
ecletica-56	150	23	mortar	mortar	NOUN
ecletica-56	150	24	.	.	PUNCT
ecletica-56	151	1	an	an	DET
ecletica-56	151	2	aliquot	aliquot	NOUN
ecletica-56	151	3	of	of	ADP
ecletica-56	151	4	the	the	DET
ecletica-56	151	5	pharmaceutical	pharmaceutical	ADJ
ecletica-56	151	6	preparation	preparation	NOUN
ecletica-56	151	7	,	,	PUNCT
ecletica-56	151	8	containing	contain	VERB
ecletica-56	151	9	c.a	c.a	PROPN
ecletica-56	151	10	.	.	PROPN
ecletica-56	152	1	500.0	500.0	NUM
ecletica-56	152	2	mg	mg	NOUN
ecletica-56	152	3	of	of	ADP
ecletica-56	152	4	metformin	metformin	NOUN
ecletica-56	152	5	hydrochloride	hydrochloride	NOUN
ecletica-56	152	6	was	be	AUX
ecletica-56	152	7	exactly	exactly	ADV
ecletica-56	152	8	weighed	weigh	VERB
ecletica-56	152	9	and	and	CCONJ
ecletica-56	152	10	transferred	transfer	VERB
ecletica-56	152	11	to	to	ADP
ecletica-56	152	12	a	a	DET
ecletica-56	152	13	100.0	100.0	NUM
ecletica-56	152	14	ml	ml	NOUN
ecletica-56	152	15	volumetric	volumetric	ADJ
ecletica-56	152	16	flask	flask	NOUN
ecletica-56	152	17	and	and	CCONJ
ecletica-56	152	18	dissolved	dissolve	VERB
ecletica-56	152	19	with	with	ADP
ecletica-56	152	20	50.0	50.0	NUM
ecletica-56	152	21	ml	ml	NOUN
ecletica-56	152	22	of	of	ADP
ecletica-56	152	23	methanol	methanol	NOUN
ecletica-56	152	24	.	.	PUNCT
ecletica-56	153	1	the	the	DET
ecletica-56	153	2	volume	volume	NOUN
ecletica-56	153	3	was	be	AUX
ecletica-56	153	4	completed	complete	VERB
ecletica-56	153	5	with	with	ADP
ecletica-56	153	6	the	the	DET
ecletica-56	153	7	ph	ph	ADJ
ecletica-56	153	8	5.00	5.00	NUM
ecletica-56	153	9	buffer	buffer	NOUN
ecletica-56	153	10	solution	solution	NOUN
ecletica-56	153	11	.	.	PUNCT
ecletica-56	154	1	from	from	ADP
ecletica-56	154	2	this	this	DET
ecletica-56	154	3	5000	5000	NUM
ecletica-56	154	4	ppm	ppm	NOUN
ecletica-56	154	5	solution	solution	NOUN
ecletica-56	154	6	2.00	2.00	NUM
ecletica-56	154	7	ml	ml	NOUN
ecletica-56	154	8	were	be	AUX
ecletica-56	154	9	taken	take	VERB
ecletica-56	154	10	and	and	CCONJ
ecletica-56	154	11	transferred	transfer	VERB
ecletica-56	154	12	to	to	ADP
ecletica-56	154	13	a	a	DET
ecletica-56	154	14	50.0	50.0	NUM
ecletica-56	154	15	ml	ml	NOUN
ecletica-56	154	16	volumetric	volumetric	NOUN
ecletica-56	154	17	balloon	balloon	NOUN
ecletica-56	154	18	.	.	PUNCT
ecletica-56	155	1	the	the	DET
ecletica-56	155	2	volume	volume	NOUN
ecletica-56	155	3	was	be	AUX
ecletica-56	155	4	completed	complete	VERB
ecletica-56	155	5	with	with	ADP
ecletica-56	155	6	the	the	DET
ecletica-56	155	7	mobile	mobile	ADJ
ecletica-56	155	8	phase	phase	NOUN
ecletica-56	155	9	above	above	ADP
ecletica-56	155	10	described	describe	VERB
ecletica-56	155	11	.	.	PUNCT
ecletica-56	156	1	from	from	ADP
ecletica-56	156	2	this	this	DET
ecletica-56	156	3	200	200	NUM
ecletica-56	156	4	ppm	ppm	NOUN
ecletica-56	156	5	solution	solution	NOUN
ecletica-56	156	6	a	a	DET
ecletica-56	156	7	140	140	NUM
ecletica-56	156	8	ppm	ppm	NOUN
ecletica-56	156	9	solution	solution	NOUN
ecletica-56	156	10	was	be	AUX
ecletica-56	156	11	prepared	prepare	VERB
ecletica-56	156	12	by	by	ADP
ecletica-56	156	13	dilution	dilution	NOUN
ecletica-56	156	14	,	,	PUNCT
ecletica-56	156	15	i.e.	i.e.	X
ecletica-56	156	16	,	,	PUNCT
ecletica-56	156	17	3.50	3.50	NUM
ecletica-56	156	18	ml	ml	NOUN
ecletica-56	156	19	were	be	AUX
ecletica-56	156	20	diluted	dilute	VERB
ecletica-56	156	21	to	to	ADP
ecletica-56	156	22	5.00	5.00	NUM
ecletica-56	156	23	ml	ml	NOUN
ecletica-56	156	24	with	with	ADP
ecletica-56	156	25	water	water	NOUN
ecletica-56	156	26	.	.	PUNCT
ecletica-56	157	1	2.4.3	2.4.3	X
ecletica-56	157	2	.	.	PUNCT
ecletica-56	157	3	sample	sample	NOUN
ecletica-56	157	4	treatment	treatment	NOUN
ecletica-56	157	5	[	[	X
ecletica-56	157	6	8	8	NUM
ecletica-56	157	7	]	]	SYM
ecletica-56	157	8	20	20	NUM
ecletica-56	157	9	tablets	tablet	NOUN
ecletica-56	157	10	were	be	AUX
ecletica-56	157	11	carefully	carefully	ADV
ecletica-56	157	12	weighed	weigh	VERB
ecletica-56	157	13	to	to	ADP
ecletica-56	157	14	0.1	0.1	NUM
ecletica-56	157	15	mg	mg	NOUN
ecletica-56	157	16	and	and	CCONJ
ecletica-56	157	17	crushed	crush	VERB
ecletica-56	157	18	in	in	ADP
ecletica-56	157	19	a	a	DET
ecletica-56	157	20	mortar	mortar	NOUN
ecletica-56	157	21	.	.	PUNCT
ecletica-56	158	1	an	an	DET
ecletica-56	158	2	aliquot	aliquot	NOUN
ecletica-56	158	3	containing	contain	VERB
ecletica-56	158	4	about	about	ADV
ecletica-56	158	5	60	60	NUM
ecletica-56	158	6	of	of	ADP
ecletica-56	158	7	metformin	metformin	NOUN
ecletica-56	158	8	was	be	AUX
ecletica-56	158	9	weighed	weigh	VERB
ecletica-56	158	10	to	to	ADP
ecletica-56	158	11	0.1	0.1	NUM
ecletica-56	158	12	mg	mg	PROPN
ecletica-56	158	13	,	,	PUNCT
ecletica-56	158	14	transferred	transfer	VERB
ecletica-56	158	15	to	to	ADP
ecletica-56	158	16	a	a	DET
ecletica-56	158	17	150	150	NUM
ecletica-56	158	18	ml	ml	NOUN
ecletica-56	158	19	beaker	beaker	NOUN
ecletica-56	158	20	and	and	CCONJ
ecletica-56	158	21	solubilized	solubilize	VERB
ecletica-56	158	22	with	with	ADP
ecletica-56	158	23	50	50	NUM
ecletica-56	158	24	ml	ml	NOUN
ecletica-56	158	25	of	of	ADP
ecletica-56	158	26	acetic	acetic	ADJ
ecletica-56	158	27	anhydride	anhydride	NOUN
ecletica-56	158	28	and	and	CCONJ
ecletica-56	158	29	4	4	NUM
ecletica-56	158	30	ml	ml	NOUN
ecletica-56	158	31	of	of	ADP
ecletica-56	158	32	formic	formic	ADJ
ecletica-56	158	33	acid	acid	PROPN
ecletica-56	158	34	.	.	PUNCT
ecletica-56	159	1	titration	titration	NOUN
ecletica-56	159	2	was	be	AUX
ecletica-56	159	3	point	point	NOUN
ecletica-56	159	4	-	-	PUNCT
ecletica-56	159	5	to	to	ADP
ecletica-56	159	6	-	-	PUNCT
ecletica-56	159	7	point	point	NOUN
ecletica-56	159	8	performed	perform	VERB
ecletica-56	159	9	with	with	ADP
ecletica-56	159	10	a	a	DET
ecletica-56	159	11	standard	standard	ADJ
ecletica-56	159	12	solution	solution	NOUN
ecletica-56	159	13	of	of	ADP
ecletica-56	159	14	perchloric	perchloric	ADJ
ecletica-56	159	15	acid	acid	NOUN
ecletica-56	159	16	0.1	0.1	NUM
ecletica-56	159	17	mol	mol	ADP
ecletica-56	159	18	l	l	NOUN
ecletica-56	159	19	-1	-1	PUNCT
ecletica-56	159	20	.	.	PUNCT
ecletica-56	160	1	methods	method	NOUN
ecletica-56	160	2	proposed	propose	VERB
ecletica-56	160	3	microgravimetric	microgravimetric	ADJ
ecletica-56	160	4	method	method	NOUN
ecletica-56	160	5	the	the	DET
ecletica-56	160	6	proposed	propose	VERB
ecletica-56	160	7	method	method	NOUN
ecletica-56	160	8	was	be	AUX
ecletica-56	160	9	based	base	VERB
ecletica-56	160	10	on	on	ADP
ecletica-56	160	11	the	the	DET
ecletica-56	160	12	reaction	reaction	NOUN
ecletica-56	160	13	of	of	ADP
ecletica-56	160	14	metformin	metformin	NOUN
ecletica-56	160	15	with	with	ADP
ecletica-56	160	16	nickel(ii	nickel(ii	PROPN
ecletica-56	160	17	)	)	PUNCT
ecletica-56	160	18	in	in	ADP
ecletica-56	160	19	aqueous	aqueous	ADJ
ecletica-56	160	20	medium	medium	NOUN
ecletica-56	160	21	forming	form	VERB
ecletica-56	160	22	an	an	DET
ecletica-56	160	23	insoluble	insoluble	ADJ
ecletica-56	160	24	complex	complex	NOUN
ecletica-56	160	25	[	[	X
ecletica-56	160	26	12	12	NUM
ecletica-56	160	27	]	]	PUNCT
ecletica-56	160	28	.	.	PUNCT
ecletica-56	161	1	the	the	DET
ecletica-56	161	2	reaction	reaction	NOUN
ecletica-56	161	3	was	be	AUX
ecletica-56	161	4	performed	perform	VERB
ecletica-56	161	5	inside	inside	ADP
ecletica-56	161	6	a	a	DET
ecletica-56	161	7	plastic	plastic	NOUN
ecletica-56	161	8	10	10	NUM
ecletica-56	161	9	ml	ml	NOUN
ecletica-56	161	10	syringe	syringe	NOUN
ecletica-56	161	11	.	.	PUNCT
ecletica-56	162	1	the	the	DET
ecletica-56	162	2	2.00	2.00	NUM
ecletica-56	162	3	ml	ml	NOUN
ecletica-56	162	4	aliquot	aliquot	NOUN
ecletica-56	162	5	of	of	ADP
ecletica-56	162	6	the	the	DET
ecletica-56	162	7	sample	sample	NOUN
ecletica-56	162	8	was	be	AUX
ecletica-56	162	9	first	first	ADV
ecletica-56	162	10	measured	measure	VERB
ecletica-56	162	11	with	with	ADP
ecletica-56	162	12	a	a	DET
ecletica-56	162	13	pipette	pipette	NOUN
ecletica-56	162	14	,	,	PUNCT
ecletica-56	162	15	placed	place	VERB
ecletica-56	162	16	in	in	ADP
ecletica-56	162	17	a	a	DET
ecletica-56	162	18	5	5	NUM
ecletica-56	162	19	ml	ml	NOUN
ecletica-56	162	20	beaker	beaker	NOUN
ecletica-56	162	21	and	and	CCONJ
ecletica-56	162	22	then	then	ADV
ecletica-56	162	23	carefully	carefully	ADV
ecletica-56	162	24	eclética	eclética	PROPN
ecletica-56	162	25	química	química	PROPN
ecletica-56	162	26	,	,	PUNCT
ecletica-56	162	27	vol	vol	NOUN
ecletica-56	162	28	.	.	PROPN
ecletica-56	162	29	40	40	NUM
ecletica-56	162	30	,	,	PUNCT
ecletica-56	162	31	62	62	NUM
ecletica-56	162	32	-	-	SYM
ecletica-56	162	33	70	70	NUM
ecletica-56	162	34	,	,	PUNCT
ecletica-56	162	35	2015	2015	NUM
ecletica-56	162	36	.	.	PUNCT
ecletica-56	163	1	65	65	NUM
ecletica-56	163	2	65	65	NUM
ecletica-56	163	3	sucked	suck	VERB
ecletica-56	163	4	with	with	ADP
ecletica-56	163	5	the	the	DET
ecletica-56	163	6	syringe	syringe	NOUN
ecletica-56	163	7	as	as	SCONJ
ecletica-56	163	8	can	can	AUX
ecletica-56	163	9	be	be	AUX
ecletica-56	163	10	saw	see	VERB
ecletica-56	163	11	in	in	ADP
ecletica-56	163	12	figure	figure	NOUN
ecletica-56	163	13	2	2	NUM
ecletica-56	163	14	.	.	PUNCT
ecletica-56	164	1	in	in	ADP
ecletica-56	164	2	sequence	sequence	NOUN
ecletica-56	164	3	the	the	DET
ecletica-56	164	4	other	other	ADJ
ecletica-56	164	5	solutions	solution	NOUN
ecletica-56	164	6	are	be	AUX
ecletica-56	164	7	successively	successively	ADV
ecletica-56	164	8	placed	place	VERB
ecletica-56	164	9	in	in	ADP
ecletica-56	164	10	this	this	DET
ecletica-56	164	11	same	same	ADJ
ecletica-56	164	12	beaker	beaker	NOUN
ecletica-56	164	13	and	and	CCONJ
ecletica-56	164	14	sucked	suck	VERB
ecletica-56	164	15	into	into	ADP
ecletica-56	164	16	the	the	DET
ecletica-56	164	17	same	same	ADJ
ecletica-56	164	18	syringe	syringe	NOUN
ecletica-56	164	19	.	.	PUNCT
ecletica-56	165	1	the	the	DET
ecletica-56	165	2	solutions	solution	NOUN
ecletica-56	165	3	were	be	AUX
ecletica-56	165	4	always	always	ADV
ecletica-56	165	5	introduced	introduce	VERB
ecletica-56	165	6	in	in	ADP
ecletica-56	165	7	the	the	DET
ecletica-56	165	8	following	follow	VERB
ecletica-56	165	9	order	order	NOUN
ecletica-56	165	10	.	.	PUNCT
ecletica-56	166	1	2.00	2.00	NUM
ecletica-56	166	2	ml	ml	NOUN
ecletica-56	166	3	sample	sample	NOUN
ecletica-56	166	4	;	;	PUNCT
ecletica-56	166	5	1.5	1.5	NUM
ecletica-56	166	6	ml	ml	NOUN
ecletica-56	166	7	nickel(ii	nickel(ii	PROPN
ecletica-56	166	8	)	)	PUNCT
ecletica-56	166	9	1.0	1.0	NUM
ecletica-56	166	10	mol	mol	ADP
ecletica-56	166	11	l	l	PROPN
ecletica-56	166	12	-1	-1	PUNCT
ecletica-56	166	13	;	;	PUNCT
ecletica-56	166	14	3.0	3.0	NUM
ecletica-56	166	15	ml	ml	NOUN
ecletica-56	166	16	nh3	nh3	NUM
ecletica-56	166	17	concentrated	concentrated	ADJ
ecletica-56	166	18	(	(	PUNCT
ecletica-56	166	19	17	17	NUM
ecletica-56	166	20	mol	mol	ADP
ecletica-56	166	21	l	l	NOUN
ecletica-56	166	22	-1	-1	PROPN
ecletica-56	166	23	)	)	PUNCT
ecletica-56	166	24	;	;	PUNCT
ecletica-56	166	25	2.0	2.0	NUM
ecletica-56	166	26	ml	ml	ADP
ecletica-56	166	27	naoh	naoh	NOUN
ecletica-56	166	28	2.0	2.0	NUM
ecletica-56	166	29	mol	mol	ADP
ecletica-56	166	30	l	l	NOUN
ecletica-56	166	31	-1	-1	PUNCT
ecletica-56	166	32	.	.	PUNCT
ecletica-56	167	1	the	the	DET
ecletica-56	167	2	precipitate	precipitate	NOUN
ecletica-56	167	3	is	be	AUX
ecletica-56	167	4	quantitatively	quantitatively	ADV
ecletica-56	167	5	formed	form	VERB
ecletica-56	167	6	in	in	ADP
ecletica-56	167	7	about	about	ADV
ecletica-56	167	8	3	3	NUM
ecletica-56	167	9	minutes	minute	NOUN
ecletica-56	167	10	(	(	PUNCT
ecletica-56	167	11	fig	fig	NOUN
ecletica-56	167	12	.	.	PUNCT
ecletica-56	168	1	3	3	NUM
ecletica-56	168	2	)	)	PUNCT
ecletica-56	168	3	.	.	PUNCT
ecletica-56	169	1	figure	figure	NOUN
ecletica-56	169	2	2	2	NUM
ecletica-56	169	3	figure	figure	NOUN
ecletica-56	169	4	3	3	NUM
ecletica-56	169	5	the	the	DET
ecletica-56	169	6	precipitate	precipitate	NOUN
ecletica-56	169	7	was	be	AUX
ecletica-56	169	8	separated	separate	VERB
ecletica-56	169	9	using	use	VERB
ecletica-56	169	10	a	a	DET
ecletica-56	169	11	tube	tube	NOUN
ecletica-56	169	12	with	with	ADP
ecletica-56	169	13	a	a	DET
ecletica-56	169	14	sintered	sinter	VERB
ecletica-56	169	15	g3	g3	NOUN
ecletica-56	169	16	glass	glass	NOUN
ecletica-56	169	17	filter	filter	NOUN
ecletica-56	170	1	[	[	X
ecletica-56	170	2	35	35	NUM
ecletica-56	170	3	]	]	X
ecletica-56	170	4	(	(	PUNCT
ecletica-56	170	5	fig	fig	NOUN
ecletica-56	170	6	.	.	PUNCT
ecletica-56	171	1	4a	4a	NOUN
ecletica-56	171	2	)	)	PUNCT
ecletica-56	171	3	or	or	CCONJ
ecletica-56	171	4	a	a	DET
ecletica-56	171	5	syringe	syringe	NOUN
ecletica-56	171	6	filter	filter	NOUN
ecletica-56	171	7	(	(	PUNCT
ecletica-56	171	8	millipore	millipore	PROPN
ecletica-56	171	9	,	,	PUNCT
ecletica-56	171	10	millex	millex	PROPN
ecletica-56	171	11	hv	hv	PROPN
ecletica-56	171	12	,	,	PUNCT
ecletica-56	171	13	0.45	0.45	NUM
ecletica-56	171	14	m	m	PROPN
ecletica-56	172	1	pore	pore	NOUN
ecletica-56	172	2	,	,	PUNCT
ecletica-56	172	3	33	33	NUM
ecletica-56	172	4	mm	mm	NOUN
ecletica-56	172	5	diameter	diameter	NOUN
ecletica-56	172	6	)	)	PUNCT
ecletica-56	172	7	(	(	PUNCT
ecletica-56	172	8	figure	figure	VERB
ecletica-56	172	9	4b	4b	PROPN
ecletica-56	172	10	)	)	PUNCT
ecletica-56	172	11	previously	previously	ADV
ecletica-56	172	12	weighed	weigh	VERB
ecletica-56	172	13	.	.	PUNCT
ecletica-56	173	1	in	in	ADP
ecletica-56	173	2	the	the	DET
ecletica-56	173	3	case	case	NOUN
ecletica-56	173	4	of	of	ADP
ecletica-56	173	5	the	the	DET
ecletica-56	173	6	glass	glass	NOUN
ecletica-56	173	7	tube	tube	NOUN
ecletica-56	173	8	vacuum	vacuum	NOUN
ecletica-56	173	9	pump	pump	NOUN
ecletica-56	173	10	was	be	AUX
ecletica-56	173	11	used	use	VERB
ecletica-56	173	12	to	to	PART
ecletica-56	173	13	filtrate	filtrate	VERB
ecletica-56	173	14	the	the	DET
ecletica-56	173	15	solid	solid	NOUN
ecletica-56	173	16	but	but	CCONJ
ecletica-56	173	17	a	a	DET
ecletica-56	173	18	centrifuge	centrifuge	NOUN
ecletica-56	173	19	can	can	AUX
ecletica-56	173	20	be	be	AUX
ecletica-56	173	21	used	use	VERB
ecletica-56	173	22	[	[	PUNCT
ecletica-56	173	23	35	35	NUM
ecletica-56	173	24	]	]	PUNCT
ecletica-56	173	25	.	.	PUNCT
ecletica-56	174	1	the	the	DET
ecletica-56	174	2	solid	solid	ADJ
ecletica-56	174	3	in	in	ADP
ecletica-56	174	4	the	the	DET
ecletica-56	174	5	filter	filter	NOUN
ecletica-56	174	6	was	be	AUX
ecletica-56	174	7	carefully	carefully	ADV
ecletica-56	174	8	washed	wash	VERB
ecletica-56	174	9	with	with	ADP
ecletica-56	174	10	about	about	ADV
ecletica-56	174	11	2.5	2.5	NUM
ecletica-56	174	12	ml	ml	NOUN
ecletica-56	174	13	of	of	ADP
ecletica-56	174	14	concentrated	concentrated	ADJ
ecletica-56	174	15	nh3	nh3	NOUN
ecletica-56	174	16	following	follow	VERB
ecletica-56	174	17	drying	dry	VERB
ecletica-56	174	18	in	in	ADP
ecletica-56	174	19	an	an	DET
ecletica-56	174	20	oven	oven	NOUN
ecletica-56	174	21	at	at	ADP
ecletica-56	174	22	120	120	NUM
ecletica-56	174	23	o	o	NOUN
ecletica-56	174	24	c	c	NOUN
ecletica-56	174	25	for	for	ADP
ecletica-56	174	26	one	one	NUM
ecletica-56	174	27	hour	hour	NOUN
ecletica-56	174	28	.	.	PUNCT
ecletica-56	175	1	from	from	ADP
ecletica-56	175	2	the	the	DET
ecletica-56	175	3	obtained	obtain	VERB
ecletica-56	175	4	weight	weight	NOUN
ecletica-56	175	5	of	of	ADP
ecletica-56	175	6	metformin	metformin	NOUN
ecletica-56	175	7	as	as	SCONJ
ecletica-56	175	8	precipitate	precipitate	VERB
ecletica-56	175	9	its	its	PRON
ecletica-56	175	10	quantity	quantity	NOUN
ecletica-56	175	11	in	in	ADP
ecletica-56	175	12	the	the	DET
ecletica-56	175	13	pharmaceutical	pharmaceutical	ADJ
ecletica-56	175	14	preparation	preparation	NOUN
ecletica-56	175	15	was	be	AUX
ecletica-56	175	16	calculated	calculate	VERB
ecletica-56	175	17	.	.	PUNCT
ecletica-56	176	1	figure	figure	VERB
ecletica-56	176	2	4	4	NUM
ecletica-56	176	3	potentiometric	potentiometric	ADJ
ecletica-56	176	4	method	method	NOUN
ecletica-56	176	5	[	[	X
ecletica-56	176	6	8,9	8,9	NUM
ecletica-56	176	7	]	]	X
ecletica-56	176	8	the	the	DET
ecletica-56	176	9	method	method	NOUN
ecletica-56	176	10	recommended	recommend	VERB
ecletica-56	176	11	by	by	ADP
ecletica-56	176	12	the	the	DET
ecletica-56	176	13	american	american	ADJ
ecletica-56	176	14	and	and	CCONJ
ecletica-56	176	15	japanese	japanese	ADJ
ecletica-56	176	16	pharmacopoeias	pharmacopoeia	NOUN
ecletica-56	176	17	was	be	AUX
ecletica-56	176	18	used	use	VERB
ecletica-56	176	19	[	[	PUNCT
ecletica-56	176	20	8,9	8,9	NUM
ecletica-56	176	21	]	]	PUNCT
ecletica-56	176	22	,	,	PUNCT
ecletica-56	176	23	using	use	VERB
ecletica-56	176	24	perchloric	perchloric	ADJ
ecletica-56	176	25	acid	acid	NOUN
ecletica-56	176	26	solution	solution	NOUN
ecletica-56	176	27	as	as	ADP
ecletica-56	176	28	titrant	titrant	NOUN
ecletica-56	176	29	.	.	PUNCT
ecletica-56	177	1	hplc	hplc	NOUN
ecletica-56	177	2	method	method	NOUN
ecletica-56	177	3	[	[	X
ecletica-56	177	4	28	28	NUM
ecletica-56	177	5	]	]	PUNCT
ecletica-56	177	6	this	this	DET
ecletica-56	177	7	procedure	procedure	NOUN
ecletica-56	177	8	is	be	AUX
ecletica-56	177	9	similar	similar	ADJ
ecletica-56	177	10	to	to	ADP
ecletica-56	177	11	that	that	PRON
ecletica-56	177	12	recommended	recommend	VERB
ecletica-56	177	13	by	by	ADP
ecletica-56	177	14	usp	usp	PROPN
ecletica-56	177	15	[	[	X
ecletica-56	177	16	8	8	NUM
ecletica-56	177	17	]	]	PUNCT
ecletica-56	177	18	,	,	PUNCT
ecletica-56	177	19	british	british	ADJ
ecletica-56	178	1	[	[	X
ecletica-56	178	2	10	10	NUM
ecletica-56	178	3	]	]	PUNCT
ecletica-56	178	4	and	and	CCONJ
ecletica-56	178	5	japanese	japanese	ADJ
ecletica-56	178	6	[	[	X
ecletica-56	178	7	9	9	NUM
ecletica-56	178	8	]	]	PUNCT
ecletica-56	178	9	pharmacopoeias	pharmacopoeia	NOUN
ecletica-56	178	10	.	.	PUNCT
ecletica-56	179	1	buffer	buffer	NOUN
ecletica-56	179	2	(	(	PUNCT
ecletica-56	179	3	nh4)h2po4	nh4)h2po4	PROPN
ecletica-56	179	4	ph=5.00	ph=5.00	PROPN
ecletica-56	179	5	and	and	CCONJ
ecletica-56	179	6	methanol	methanol	VERB
ecletica-56	179	7	50:50	50:50	NUM
ecletica-56	179	8	v	v	NOUN
ecletica-56	179	9	/	/	SYM
ecletica-56	179	10	v	v	NOUN
ecletica-56	179	11	as	as	SCONJ
ecletica-56	179	12	mobile	mobile	ADJ
ecletica-56	179	13	phase	phase	NOUN
ecletica-56	179	14	was	be	AUX
ecletica-56	179	15	used	use	VERB
ecletica-56	179	16	at	at	ADP
ecletica-56	179	17	1	1	NUM
ecletica-56	179	18	ml	ml	NOUN
ecletica-56	179	19	min	min	PROPN
ecletica-56	179	20	-1	-1	INTJ
ecletica-56	179	21	.	.	PUNCT
ecletica-56	180	1	the	the	DET
ecletica-56	180	2	column	column	NOUN
ecletica-56	180	3	(	(	PUNCT
ecletica-56	180	4	300	300	NUM
ecletica-56	180	5			NOUN
ecletica-56	180	6	3.0	3.0	NUM
ecletica-56	180	7	mm	mm	NOUN
ecletica-56	180	8	)	)	PUNCT
ecletica-56	180	9	was	be	AUX
ecletica-56	180	10	a	a	DET
ecletica-56	180	11	microbondapack	microbondapack	NOUN
ecletica-56	180	12	c18	c18	NOUN
ecletica-56	180	13	waters	water	NOUN
ecletica-56	180	14	,	,	PUNCT
ecletica-56	180	15	10	10	NUM
ecletica-56	180	16	m	m	PROPN
ecletica-56	180	17	diameter	diameter	NOUN
ecletica-56	180	18	particle	particle	NOUN
ecletica-56	180	19	size	size	NOUN
ecletica-56	180	20	;	;	PUNCT
ecletica-56	180	21	temperature	temperature	NOUN
ecletica-56	180	22	40	40	NUM
ecletica-56	180	23	o	o	NOUN
ecletica-56	180	24	c	c	X
ecletica-56	180	25	,	,	PUNCT
ecletica-56	180	26	λmax	λmax	NOUN
ecletica-56	180	27	225	225	NUM
ecletica-56	180	28	nm	nm	ADJ
ecletica-56	180	29	and	and	CCONJ
ecletica-56	180	30	injection	injection	NOUN
ecletica-56	180	31	volume	volume	NOUN
ecletica-56	180	32	20	20	NUM
ecletica-56	180	33	μl	μl	NOUN
ecletica-56	180	34	.	.	PUNCT
ecletica-56	181	1	statistical	statistical	ADJ
ecletica-56	181	2	treatment	treatment	NOUN
ecletica-56	181	3	for	for	ADP
ecletica-56	181	4	statistical	statistical	ADJ
ecletica-56	181	5	comparison	comparison	NOUN
ecletica-56	181	6	of	of	ADP
ecletica-56	181	7	the	the	DET
ecletica-56	181	8	data	datum	NOUN
ecletica-56	181	9	obtained	obtain	VERB
ecletica-56	181	10	with	with	ADP
ecletica-56	181	11	the	the	DET
ecletica-56	181	12	proposed	propose	VERB
ecletica-56	181	13	method	method	NOUN
ecletica-56	181	14	versus	versus	ADP
ecletica-56	181	15	the	the	DET
ecletica-56	181	16	reference	reference	NOUN
ecletica-56	181	17	methods	method	VERB
ecletica-56	181	18	the	the	DET
ecletica-56	181	19	t	t	PROPN
ecletica-56	181	20	test	test	NOUN
ecletica-56	181	21	of	of	ADP
ecletica-56	181	22	student	student	NOUN
ecletica-56	181	23	and	and	CCONJ
ecletica-56	181	24	the	the	DET
ecletica-56	181	25	snedecor	snedecor	NOUN
ecletica-56	181	26	f	f	PROPN
ecletica-56	181	27	test	test	NOUN
ecletica-56	181	28	were	be	AUX
ecletica-56	181	29	used	use	VERB
ecletica-56	181	30	[	[	PUNCT
ecletica-56	181	31	36	36	NUM
ecletica-56	181	32	]	]	PUNCT
ecletica-56	181	33	.	.	PUNCT
ecletica-56	182	1	results	result	NOUN
ecletica-56	182	2	and	and	CCONJ
ecletica-56	182	3	discussion	discussion	VERB
ecletica-56	182	4	the	the	DET
ecletica-56	182	5	orange	orange	PROPN
ecletica-56	182	6	color	color	NOUN
ecletica-56	182	7	precipitate	precipitate	NOUN
ecletica-56	182	8	of	of	ADP
ecletica-56	182	9	nickel	nickel	NOUN
ecletica-56	182	10	-	-	PUNCT
ecletica-56	182	11	metformin	metformin	NOUN
ecletica-56	182	12	complex	complex	NOUN
ecletica-56	182	13	is	be	AUX
ecletica-56	182	14	easily	easily	ADV
ecletica-56	182	15	formed	form	VERB
ecletica-56	182	16	but	but	CCONJ
ecletica-56	182	17	the	the	DET
ecletica-56	182	18	solution	solution	NOUN
ecletica-56	182	19	must	must	AUX
ecletica-56	182	20	be	be	AUX
ecletica-56	182	21	strictly	strictly	ADV
ecletica-56	182	22	mixed	mix	VERB
ecletica-56	182	23	in	in	ADP
ecletica-56	182	24	the	the	DET
ecletica-56	182	25	indicated	indicate	VERB
ecletica-56	182	26	order	order	NOUN
ecletica-56	182	27	:	:	PUNCT
ecletica-56	182	28	metformin	metformin	NOUN
ecletica-56	182	29	,	,	PUNCT
ecletica-56	182	30	nickel	nickel	NOUN
ecletica-56	182	31	,	,	PUNCT
ecletica-56	182	32	ammonium	ammonium	NOUN
ecletica-56	182	33	hydroxide	hydroxide	NOUN
ecletica-56	182	34	,	,	PUNCT
ecletica-56	182	35	sodium	sodium	NOUN
ecletica-56	182	36	hydroxide	hydroxide	NOUN
ecletica-56	182	37	.	.	PUNCT
ecletica-56	183	1	mainly	mainly	ADV
ecletica-56	183	2	in	in	ADP
ecletica-56	183	3	the	the	DET
ecletica-56	183	4	case	case	NOUN
ecletica-56	183	5	of	of	ADP
ecletica-56	183	6	sodium	sodium	NOUN
ecletica-56	183	7	hydroxide	hydroxide	NOUN
ecletica-56	183	8	solution	solution	NOUN
ecletica-56	183	9	that	that	PRON
ecletica-56	183	10	is	be	AUX
ecletica-56	183	11	added	add	VERB
ecletica-56	183	12	in	in	ADP
ecletica-56	183	13	order	order	NOUN
ecletica-56	183	14	to	to	PART
ecletica-56	183	15	increase	increase	VERB
ecletica-56	183	16	the	the	DET
ecletica-56	183	17	ph	ph	NOUN
ecletica-56	183	18	,	,	PUNCT
ecletica-56	183	19	if	if	SCONJ
ecletica-56	183	20	it	it	PRON
ecletica-56	183	21	is	be	AUX
ecletica-56	183	22	mixed	mixed	ADJ
ecletica-56	183	23	before	before	SCONJ
ecletica-56	183	24	the	the	DET
ecletica-56	183	25	ammonium	ammonium	NOUN
ecletica-56	183	26	hydroxide	hydroxide	NOUN
ecletica-56	183	27	,	,	PUNCT
ecletica-56	183	28	nickel	nickel	NOUN
ecletica-56	183	29	hydroxide	hydroxide	NOUN
ecletica-56	183	30	precipitates	precipitate	NOUN
ecletica-56	183	31	and	and	CCONJ
ecletica-56	183	32	the	the	DET
ecletica-56	183	33	formation	formation	NOUN
ecletica-56	183	34	of	of	ADP
ecletica-56	183	35	the	the	DET
ecletica-56	183	36	desired	desire	VERB
ecletica-56	183	37	complex	complex	NOUN
ecletica-56	183	38	does	do	AUX
ecletica-56	183	39	not	not	PART
ecletica-56	183	40	occur	occur	VERB
ecletica-56	183	41	.	.	PUNCT
ecletica-56	184	1	it	it	PRON
ecletica-56	184	2	is	be	AUX
ecletica-56	184	3	important	important	ADJ
ecletica-56	184	4	to	to	PART
ecletica-56	184	5	pay	pay	VERB
ecletica-56	184	6	attention	attention	NOUN
ecletica-56	184	7	to	to	ADP
ecletica-56	184	8	the	the	DET
ecletica-56	184	9	molar	molar	ADJ
ecletica-56	184	10	excess	excess	NOUN
ecletica-56	184	11	of	of	ADP
ecletica-56	184	12	nickel	nickel	NOUN
ecletica-56	184	13	,	,	PUNCT
ecletica-56	184	14	with	with	ADP
ecletica-56	184	15	respect	respect	NOUN
ecletica-56	184	16	to	to	ADP
ecletica-56	184	17	metformin	metformin	NOUN
ecletica-56	184	18	(	(	PUNCT
ecletica-56	184	19	mf	mf	NOUN
ecletica-56	184	20	)	)	PUNCT
ecletica-56	184	21	,	,	PUNCT
ecletica-56	184	22	in	in	ADP
ecletica-56	184	23	eclética	eclética	PROPN
ecletica-56	184	24	química	química	PROPN
ecletica-56	184	25	,	,	PUNCT
ecletica-56	184	26	vol	vol	NOUN
ecletica-56	184	27	.	.	PROPN
ecletica-56	184	28	40	40	NUM
ecletica-56	184	29	,	,	PUNCT
ecletica-56	184	30	62	62	NUM
ecletica-56	184	31	-	-	SYM
ecletica-56	184	32	70	70	NUM
ecletica-56	184	33	,	,	PUNCT
ecletica-56	184	34	2015	2015	NUM
ecletica-56	184	35	.	.	PUNCT
ecletica-56	185	1	66	66	NUM
ecletica-56	185	2	66	66	NUM
ecletica-56	185	3	order	order	NOUN
ecletica-56	185	4	to	to	PART
ecletica-56	185	5	guarantee	guarantee	VERB
ecletica-56	185	6	the	the	DET
ecletica-56	185	7	quantitative	quantitative	ADJ
ecletica-56	185	8	formation	formation	NOUN
ecletica-56	185	9	of	of	ADP
ecletica-56	185	10	the	the	DET
ecletica-56	185	11	complex	complex	NOUN
ecletica-56	185	12	.	.	PUNCT
ecletica-56	186	1	the	the	DET
ecletica-56	186	2	solution	solution	NOUN
ecletica-56	186	3	of	of	ADP
ecletica-56	186	4	metformin	metformin	NOUN
ecletica-56	186	5	presents	present	VERB
ecletica-56	186	6	no	no	DET
ecletica-56	186	7	color	color	NOUN
ecletica-56	186	8	,	,	PUNCT
ecletica-56	186	9	unless	unless	SCONJ
ecletica-56	186	10	an	an	DET
ecletica-56	186	11	organic	organic	ADJ
ecletica-56	186	12	colorant	colorant	NOUN
ecletica-56	186	13	is	be	AUX
ecletica-56	186	14	present	present	ADJ
ecletica-56	186	15	.	.	PUNCT
ecletica-56	187	1	the	the	DET
ecletica-56	187	2	addition	addition	NOUN
ecletica-56	187	3	of	of	ADP
ecletica-56	187	4	the	the	DET
ecletica-56	187	5	green	green	ADJ
ecletica-56	187	6	solution	solution	NOUN
ecletica-56	187	7	of	of	ADP
ecletica-56	187	8	ni(ii	ni(ii	PROPN
ecletica-56	187	9	)	)	PUNCT
ecletica-56	187	10	turns	turn	VERB
ecletica-56	187	11	all	all	DET
ecletica-56	187	12	solution	solution	NOUN
ecletica-56	187	13	in	in	ADP
ecletica-56	187	14	this	this	DET
ecletica-56	187	15	color	color	NOUN
ecletica-56	187	16	.	.	PUNCT
ecletica-56	188	1	the	the	DET
ecletica-56	188	2	addition	addition	NOUN
ecletica-56	188	3	of	of	ADP
ecletica-56	188	4	the	the	DET
ecletica-56	188	5	ammonium	ammonium	NOUN
ecletica-56	188	6	hydroxide	hydroxide	NOUN
ecletica-56	188	7	causes	cause	VERB
ecletica-56	188	8	change	change	NOUN
ecletica-56	188	9	to	to	ADP
ecletica-56	188	10	a	a	DET
ecletica-56	188	11	blue	blue	ADJ
ecletica-56	188	12	color	color	NOUN
ecletica-56	188	13	as	as	ADP
ecletica-56	188	14	the	the	DET
ecletica-56	188	15	result	result	NOUN
ecletica-56	188	16	of	of	ADP
ecletica-56	188	17	the	the	DET
ecletica-56	188	18	ni(nh3)6	ni(nh3)6	NOUN
ecletica-56	188	19	2	2	NUM
ecletica-56	188	20	+	+	NUM
ecletica-56	188	21	hexamine	hexamine	NOUN
ecletica-56	188	22	complex	complex	NOUN
ecletica-56	188	23	.	.	PUNCT
ecletica-56	189	1	with	with	ADP
ecletica-56	189	2	the	the	DET
ecletica-56	189	3	posterior	posterior	ADJ
ecletica-56	189	4	sodium	sodium	NOUN
ecletica-56	189	5	hydroxide	hydroxide	NOUN
ecletica-56	189	6	solution	solution	NOUN
ecletica-56	189	7	an	an	DET
ecletica-56	189	8	orange	orange	ADJ
ecletica-56	189	9	species	specie	NOUN
ecletica-56	189	10	is	be	AUX
ecletica-56	189	11	formed	form	VERB
ecletica-56	189	12	in	in	ADP
ecletica-56	189	13	solution	solution	NOUN
ecletica-56	189	14	,	,	PUNCT
ecletica-56	189	15	precipitating	precipitate	VERB
ecletica-56	189	16	soon	soon	ADV
ecletica-56	189	17	after	after	ADV
ecletica-56	189	18	as	as	ADP
ecletica-56	189	19	ni(mf)2	ni(mf)2	NOUN
ecletica-56	189	20	.	.	PUNCT
ecletica-56	190	1	the	the	DET
ecletica-56	190	2	sodium	sodium	NOUN
ecletica-56	190	3	hydroxide	hydroxide	NOUN
ecletica-56	190	4	solution	solution	NOUN
ecletica-56	190	5	must	must	AUX
ecletica-56	190	6	be	be	AUX
ecletica-56	190	7	slowly	slowly	ADV
ecletica-56	190	8	and	and	CCONJ
ecletica-56	190	9	in	in	ADP
ecletica-56	190	10	three	three	NUM
ecletica-56	190	11	portions	portion	NOUN
ecletica-56	190	12	so	so	SCONJ
ecletica-56	190	13	the	the	DET
ecletica-56	190	14	precipitate	precipitate	NOUN
ecletica-56	190	15	will	will	AUX
ecletica-56	190	16	be	be	AUX
ecletica-56	190	17	gradually	gradually	ADV
ecletica-56	190	18	formed	form	VERB
ecletica-56	190	19	.	.	PUNCT
ecletica-56	191	1	as	as	SCONJ
ecletica-56	191	2	the	the	DET
ecletica-56	191	3	ammonia	ammonia	NOUN
ecletica-56	191	4	complexes	complex	NOUN
ecletica-56	191	5	with	with	ADP
ecletica-56	191	6	ni(ii	ni(ii	NOUN
ecletica-56	191	7	)	)	PUNCT
ecletica-56	191	8	,	,	PUNCT
ecletica-56	191	9	forming	form	VERB
ecletica-56	191	10	the	the	DET
ecletica-56	191	11	hexamine	hexamine	NOUN
ecletica-56	191	12	complex	complex	NOUN
ecletica-56	191	13	a	a	DET
ecletica-56	191	14	soluble	soluble	ADJ
ecletica-56	191	15	species	specie	NOUN
ecletica-56	191	16	,	,	PUNCT
ecletica-56	191	17	the	the	DET
ecletica-56	191	18	precipitation	precipitation	NOUN
ecletica-56	191	19	of	of	ADP
ecletica-56	191	20	nickel	nickel	NOUN
ecletica-56	191	21	as	as	ADP
ecletica-56	191	22	hydroxide	hydroxide	NOUN
ecletica-56	191	23	when	when	SCONJ
ecletica-56	191	24	sodium	sodium	NOUN
ecletica-56	191	25	hydroxide	hydroxide	NOUN
ecletica-56	191	26	is	be	AUX
ecletica-56	191	27	added	add	VERB
ecletica-56	191	28	is	be	AUX
ecletica-56	191	29	avoided	avoid	VERB
ecletica-56	191	30	and	and	CCONJ
ecletica-56	191	31	he	he	PRON
ecletica-56	191	32	excess	excess	ADV
ecletica-56	191	33	of	of	ADP
ecletica-56	191	34	this	this	DET
ecletica-56	191	35	cation	cation	NOUN
ecletica-56	191	36	can	can	AUX
ecletica-56	191	37	be	be	AUX
ecletica-56	191	38	easily	easily	ADV
ecletica-56	191	39	removed	remove	VERB
ecletica-56	191	40	by	by	ADP
ecletica-56	191	41	washing	wash	VERB
ecletica-56	191	42	the	the	DET
ecletica-56	191	43	precipitate	precipitate	NOUN
ecletica-56	191	44	with	with	ADP
ecletica-56	191	45	the	the	DET
ecletica-56	191	46	concentrated	concentrate	VERB
ecletica-56	191	47	ammonium	ammonium	NOUN
ecletica-56	191	48	hydroxide	hydroxide	NOUN
ecletica-56	191	49	.	.	PUNCT
ecletica-56	192	1	the	the	DET
ecletica-56	192	2	remainder	remainder	NOUN
ecletica-56	192	3	ammonia	ammonia	NOUN
ecletica-56	192	4	in	in	ADP
ecletica-56	192	5	the	the	DET
ecletica-56	192	6	precipitate	precipitate	NOUN
ecletica-56	192	7	can	can	AUX
ecletica-56	192	8	be	be	AUX
ecletica-56	192	9	easily	easily	ADV
ecletica-56	192	10	eliminated	eliminate	VERB
ecletica-56	192	11	by	by	ADP
ecletica-56	192	12	heating	heat	VERB
ecletica-56	192	13	in	in	ADP
ecletica-56	192	14	an	an	DET
ecletica-56	192	15	oven	oven	NOUN
ecletica-56	192	16	at	at	ADP
ecletica-56	192	17	120	120	NUM
ecletica-56	192	18	o	o	NOUN
ecletica-56	192	19	c.	c.	NOUN
ecletica-56	192	20	the	the	DET
ecletica-56	192	21	reaction	reaction	NOUN
ecletica-56	192	22	of	of	ADP
ecletica-56	192	23	formation	formation	NOUN
ecletica-56	192	24	of	of	ADP
ecletica-56	192	25	the	the	DET
ecletica-56	192	26	ni(mf)2	ni(mf)2	NOUN
ecletica-56	192	27	complex	complex	NOUN
ecletica-56	192	28	,	,	PUNCT
ecletica-56	192	29	which	which	PRON
ecletica-56	192	30	precipitates	precipitate	VERB
ecletica-56	192	31	as	as	ADP
ecletica-56	192	32	an	an	DET
ecletica-56	192	33	orange	orange	ADJ
ecletica-56	192	34	color	color	NOUN
ecletica-56	192	35	solid	solid	ADJ
ecletica-56	192	36	,	,	PUNCT
ecletica-56	192	37	can	can	AUX
ecletica-56	192	38	be	be	AUX
ecletica-56	192	39	summarized	summarize	VERB
ecletica-56	192	40	by	by	ADP
ecletica-56	192	41	the	the	DET
ecletica-56	192	42	following	follow	VERB
ecletica-56	192	43	equation	equation	NOUN
ecletica-56	192	44	which	which	PRON
ecletica-56	192	45	clearly	clearly	ADV
ecletica-56	192	46	shows	show	VERB
ecletica-56	192	47	the	the	DET
ecletica-56	192	48	necessity	necessity	NOUN
ecletica-56	192	49	of	of	ADP
ecletica-56	192	50	a	a	DET
ecletica-56	192	51	base	base	NOUN
ecletica-56	192	52	to	to	PART
ecletica-56	192	53	shift	shift	VERB
ecletica-56	192	54	reaction	reaction	NOUN
ecletica-56	192	55	to	to	ADP
ecletica-56	192	56	the	the	DET
ecletica-56	192	57	right	right	NOUN
ecletica-56	192	58	:	:	PUNCT
ecletica-56	192	59	2	2	NUM
ecletica-56	192	60	c4h11n5	c4h11n5	NOUN
ecletica-56	192	61	+	+	CCONJ
ecletica-56	192	62	ni	ni	PROPN
ecletica-56	192	63	2	2	NUM
ecletica-56	192	64	+	+	PROPN
ecletica-56	192	65	→	→	SYM
ecletica-56	192	66	ni(c4h10n5)2(s	ni(c4h10n5)2(s	NOUN
ecletica-56	192	67	)	)	PUNCT
ecletica-56	193	1	+	+	CCONJ
ecletica-56	193	2	2	2	NUM
ecletica-56	193	3	h	h	NOUN
ecletica-56	193	4	+	+	CCONJ
ecletica-56	193	5	a	a	DET
ecletica-56	193	6	glass	glass	NOUN
ecletica-56	193	7	tube	tube	NOUN
ecletica-56	193	8	containing	contain	VERB
ecletica-56	193	9	a	a	DET
ecletica-56	193	10	g3	g3	NOUN
ecletica-56	193	11	porosity	porosity	NOUN
ecletica-56	193	12	sintered	sinter	VERB
ecletica-56	193	13	glass	glass	NOUN
ecletica-56	193	14	disc	disc	NOUN
ecletica-56	193	15	35	35	NUM
ecletica-56	193	16	was	be	AUX
ecletica-56	193	17	used	use	VERB
ecletica-56	193	18	to	to	PART
ecletica-56	193	19	filter	filter	VERB
ecletica-56	193	20	the	the	DET
ecletica-56	193	21	precipitate	precipitate	NOUN
ecletica-56	193	22	or	or	CCONJ
ecletica-56	193	23	alternatively	alternatively	ADV
ecletica-56	193	24	a	a	DET
ecletica-56	193	25	millipore	millipore	PROPN
ecletica-56	193	26	syringe	syringe	PROPN
ecletica-56	193	27	filter	filter	NOUN
ecletica-56	193	28	(	(	PUNCT
ecletica-56	193	29	millipore	millipore	PROPN
ecletica-56	193	30	,	,	PUNCT
ecletica-56	193	31	millex	millex	PROPN
ecletica-56	193	32	hv	hv	PROPN
ecletica-56	193	33	,	,	PUNCT
ecletica-56	194	1	0.45	0.45	NUM
ecletica-56	194	2	m	m	PROPN
ecletica-56	194	3	pore	pore	NOUN
ecletica-56	194	4	,	,	PUNCT
ecletica-56	194	5	33	33	NUM
ecletica-56	194	6	mm	mm	NOUN
ecletica-56	194	7	diameter	diameter	NOUN
ecletica-56	194	8	)	)	PUNCT
ecletica-56	194	9	.	.	PUNCT
ecletica-56	195	1	the	the	DET
ecletica-56	195	2	same	same	ADJ
ecletica-56	195	3	samples	sample	NOUN
ecletica-56	195	4	were	be	AUX
ecletica-56	195	5	analized	analize	VERB
ecletica-56	195	6	using	use	VERB
ecletica-56	195	7	the	the	DET
ecletica-56	195	8	titrimetric	titrimetric	ADJ
ecletica-56	195	9	potenciometric	potenciometric	ADJ
ecletica-56	195	10	procedure	procedure	NOUN
ecletica-56	195	11	recommended	recommend	VERB
ecletica-56	195	12	by	by	ADP
ecletica-56	195	13	pharmacopeias	pharmacopeia	NOUN
ecletica-56	195	14	[	[	X
ecletica-56	195	15	8,9	8,9	X
ecletica-56	195	16	]	]	PUNCT
ecletica-56	195	17	and	and	CCONJ
ecletica-56	195	18	by	by	ADP
ecletica-56	195	19	a	a	DET
ecletica-56	195	20	hplc	hplc	NOUN
ecletica-56	195	21	method	method	NOUN
ecletica-56	195	22	[	[	X
ecletica-56	195	23	28	28	NUM
ecletica-56	195	24	]	]	PUNCT
ecletica-56	195	25	.	.	PUNCT
ecletica-56	196	1	this	this	DET
ecletica-56	196	2	last	last	ADJ
ecletica-56	196	3	procedure	procedure	NOUN
ecletica-56	196	4	was	be	AUX
ecletica-56	196	5	preferred	prefer	VERB
ecletica-56	196	6	as	as	SCONJ
ecletica-56	196	7	it	it	PRON
ecletica-56	196	8	uses	use	VERB
ecletica-56	196	9	external	external	ADJ
ecletica-56	196	10	standard	standard	NOUN
ecletica-56	196	11	.	.	PUNCT
ecletica-56	197	1	all	all	DET
ecletica-56	197	2	the	the	DET
ecletica-56	197	3	essays	essay	NOUN
ecletica-56	197	4	were	be	AUX
ecletica-56	197	5	done	do	VERB
ecletica-56	197	6	in	in	ADP
ecletica-56	197	7	triplicate	triplicate	NOUN
ecletica-56	197	8	.	.	PUNCT
ecletica-56	198	1	table	table	NOUN
ecletica-56	198	2	1	1	NUM
ecletica-56	198	3	.	.	PUNCT
ecletica-56	198	4	comparison	comparison	NOUN
ecletica-56	198	5	of	of	ADP
ecletica-56	198	6	the	the	DET
ecletica-56	198	7	determination	determination	NOUN
ecletica-56	198	8	of	of	ADP
ecletica-56	198	9	metformin	metformin	NOUN
ecletica-56	198	10	hydrochloride	hydrochloride	NOUN
ecletica-56	198	11	in	in	ADP
ecletica-56	198	12	pharmaceutical	pharmaceutical	ADJ
ecletica-56	198	13	preparations	preparation	NOUN
ecletica-56	198	14	using	use	VERB
ecletica-56	198	15	the	the	DET
ecletica-56	198	16	proposed	propose	VERB
ecletica-56	198	17	method	method	NOUN
ecletica-56	198	18	,	,	PUNCT
ecletica-56	198	19	hplc[28	hplc[28	X
ecletica-56	198	20	]	]	PUNCT
ecletica-56	198	21	and	and	CCONJ
ecletica-56	198	22	that	that	PRON
ecletica-56	198	23	of	of	ADP
ecletica-56	198	24	potentiometric	potentiometric	ADJ
ecletica-56	198	25	titration	titration	NOUN
ecletica-56	198	26	according	according	ADP
ecletica-56	198	27	pharmacopoeias[8,9	pharmacopoeias[8,9	PROPN
ecletica-56	198	28	]	]	PUNCT
ecletica-56	198	29	.	.	PUNCT
ecletica-56	199	1	values	value	NOUN
ecletica-56	199	2	are	be	AUX
ecletica-56	199	3	in	in	ADP
ecletica-56	199	4	milligrams	milligram	NOUN
ecletica-56	199	5	per	per	ADP
ecletica-56	199	6	tablet	tablet	NOUN
ecletica-56	199	7			PROPN
ecletica-56	199	8	sd	sd	PROPN
ecletica-56	199	9	.	.	PUNCT
ecletica-56	200	1	sample	sample	PROPN
ecletica-56	200	2	label	label	NOUN
ecletica-56	200	3	grav	grav	PROPN
ecletica-56	200	4	.	.	PUNCT
ecletica-56	201	1	t	t	PROPN
ecletica-56	201	2	grav	grav	PROPN
ecletica-56	201	3	.	.	PUNCT
ecletica-56	202	1	f	f	PROPN
ecletica-56	202	2	hplc	hplc	PROPN
ecletica-56	202	3	official	official	NOUN
ecletica-56	202	4	i	i	PRON
ecletica-56	202	5	a	a	DET
ecletica-56	202	6	850	850	NUM
ecletica-56	202	7	841.31.7	841.31.7	NUM
ecletica-56	202	8	841.77.5	841.77.5	NUM
ecletica-56	202	9	870.115.1	870.115.1	NUM
ecletica-56	202	10	852.25.5	852.25.5	NUM
ecletica-56	202	11	rsd	rsd	NOUN
ecletica-56	202	12	(	(	PUNCT
ecletica-56	202	13	%	%	NOUN
ecletica-56	202	14	)	)	PUNCT
ecletica-56	202	15	0.2	0.2	NUM
ecletica-56	202	16	0.9	0.9	NUM
ecletica-56	202	17	1.7	1.7	NUM
ecletica-56	202	18	0.6	0.6	NUM
ecletica-56	202	19	ii	ii	PROPN
ecletica-56	202	20	b	b	X
ecletica-56	202	21	500	500	NUM
ecletica-56	202	22	490.22.4	490.22.4	NUM
ecletica-56	202	23	492.99.0	492.99.0	NOUN
ecletica-56	203	1	511.52.9	511.52.9	NUM
ecletica-56	203	2	499.94.5	499.94.5	PROPN
ecletica-56	203	3	rsd	rsd	NOUN
ecletica-56	203	4	(	(	PUNCT
ecletica-56	203	5	%	%	NOUN
ecletica-56	203	6	)	)	PUNCT
ecletica-56	203	7	0.5	0.5	NUM
ecletica-56	203	8	1.8	1.8	NUM
ecletica-56	203	9	0.6	0.6	NUM
ecletica-56	203	10	0.9	0.9	NUM
ecletica-56	203	11	a	a	DET
ecletica-56	203	12	the	the	DET
ecletica-56	203	13	tablet	tablet	NOUN
ecletica-56	203	14	also	also	ADV
ecletica-56	203	15	contains	contain	VERB
ecletica-56	203	16	microcrystalline	microcrystalline	NOUN
ecletica-56	203	17	cellulose	cellulose	NOUN
ecletica-56	203	18	,	,	PUNCT
ecletica-56	203	19	crospovidone	crospovidone	NOUN
ecletica-56	203	20	,	,	PUNCT
ecletica-56	203	21	colloidal	colloidal	NOUN
ecletica-56	203	22	silicon	silicon	NOUN
ecletica-56	203	23	dioxide	dioxide	NOUN
ecletica-56	203	24	,	,	PUNCT
ecletica-56	203	25	magnesium	magnesium	NOUN
ecletica-56	203	26	stearate	stearate	NOUN
ecletica-56	203	27	,	,	PUNCT
ecletica-56	203	28	polyvinylpyrrolidone	polyvinylpyrrolidone	NOUN
ecletica-56	203	29	,	,	PUNCT
ecletica-56	203	30	croscarmelose	croscarmelose	ADJ
ecletica-56	203	31	sodium	sodium	NOUN
ecletica-56	203	32	,	,	PUNCT
ecletica-56	203	33	sodium	sodium	NOUN
ecletica-56	203	34	starch	starch	NOUN
ecletica-56	203	35	glycolate	glycolate	NOUN
ecletica-56	203	36	.	.	PUNCT
ecletica-56	204	1	b	b	X
ecletica-56	204	2	the	the	DET
ecletica-56	204	3	tablet	tablet	NOUN
ecletica-56	204	4	also	also	ADV
ecletica-56	204	5	contains	contain	VERB
ecletica-56	204	6	microcrystalline	microcrystalline	NOUN
ecletica-56	204	7	cellulose	cellulose	NOUN
ecletica-56	204	8	,	,	PUNCT
ecletica-56	204	9	crospovidone	crospovidone	NOUN
ecletica-56	204	10	,	,	PUNCT
ecletica-56	204	11	colloidal	colloidal	NOUN
ecletica-56	204	12	silicon	silicon	NOUN
ecletica-56	204	13	dioxide	dioxide	NOUN
ecletica-56	204	14	,	,	PUNCT
ecletica-56	204	15	magnesium	magnesium	NOUN
ecletica-56	204	16	stearate	stearate	NOUN
ecletica-56	204	17	,	,	PUNCT
ecletica-56	204	18	povidone	povidone	NOUN
ecletica-56	204	19	,	,	PUNCT
ecletica-56	204	20	hypromellose	hypromellose	NOUN
ecletica-56	204	21	,	,	PUNCT
ecletica-56	204	22	polyethylene	polyethylene	NOUN
ecletica-56	204	23	glycol	glycol	NOUN
ecletica-56	204	24	.	.	PUNCT
ecletica-56	205	1	grav	grav	PROPN
ecletica-56	205	2	.	.	PUNCT
ecletica-56	206	1	t	t	PROPN
ecletica-56	206	2	=	=	PUNCT
ecletica-56	206	3	proposed	propose	VERB
ecletica-56	206	4	gravimetric	gravimetric	NOUN
ecletica-56	206	5	;	;	PUNCT
ecletica-56	206	6	filtration	filtration	NOUN
ecletica-56	206	7	using	use	VERB
ecletica-56	206	8	glass	glass	NOUN
ecletica-56	206	9	tubes	tube	NOUN
ecletica-56	206	10	with	with	ADP
ecletica-56	206	11	sintered	sinter	VERB
ecletica-56	206	12	disc	disc	NOUN
ecletica-56	206	13	(	(	PUNCT
ecletica-56	206	14	n=3	n=3	NOUN
ecletica-56	206	15	)	)	PUNCT
ecletica-56	206	16	.	.	PUNCT
ecletica-56	207	1	grav	grav	PROPN
ecletica-56	207	2	.	.	PUNCT
ecletica-56	208	1	t	t	PROPN
ecletica-56	208	2	=	=	PUNCT
ecletica-56	208	3	proposed	propose	VERB
ecletica-56	208	4	gravimetric	gravimetric	NOUN
ecletica-56	208	5	;	;	PUNCT
ecletica-56	208	6	filtration	filtration	NOUN
ecletica-56	208	7	using	use	VERB
ecletica-56	208	8	syringe	syringe	NOUN
ecletica-56	208	9	filters	filter	NOUN
ecletica-56	208	10	(	(	PUNCT
ecletica-56	208	11	n=3	n=3	NOUN
ecletica-56	208	12	)	)	PUNCT
ecletica-56	208	13	.	.	PUNCT
ecletica-56	209	1	hplc	hplc	NOUN
ecletica-56	209	2	=	=	SYM
ecletica-56	209	3	high	high	ADJ
ecletica-56	209	4	pressure	pressure	NOUN
ecletica-56	209	5	liquid	liquid	NOUN
ecletica-56	209	6	chromatography	chromatography	NOUN
ecletica-56	209	7	(	(	PUNCT
ecletica-56	209	8	n=3	n=3	NOUN
ecletica-56	209	9	)	)	PUNCT
ecletica-56	209	10	.	.	PUNCT
ecletica-56	210	1	official	official	ADJ
ecletica-56	210	2	=	=	SYM
ecletica-56	210	3	potentiomettric	potentiomettric	PROPN
ecletica-56	210	4	titration	titration	NOUN
ecletica-56	210	5	(	(	PUNCT
ecletica-56	210	6	n=3	n=3	NOUN
ecletica-56	210	7	)	)	PUNCT
ecletica-56	210	8	.	.	PUNCT
ecletica-56	211	1	eclética	eclética	PROPN
ecletica-56	211	2	química	química	PROPN
ecletica-56	211	3	,	,	PUNCT
ecletica-56	211	4	vol	vol	NOUN
ecletica-56	211	5	.	.	PROPN
ecletica-56	211	6	40	40	NUM
ecletica-56	211	7	,	,	PUNCT
ecletica-56	211	8	62	62	NUM
ecletica-56	211	9	-	-	SYM
ecletica-56	211	10	70	70	NUM
ecletica-56	211	11	,	,	PUNCT
ecletica-56	211	12	2015	2015	NUM
ecletica-56	211	13	.	.	PUNCT
ecletica-56	212	1	67	67	NUM
ecletica-56	212	2	67	67	NUM
ecletica-56	212	3	the	the	DET
ecletica-56	212	4	results	result	NOUN
ecletica-56	212	5	shown	show	VERB
ecletica-56	212	6	in	in	ADP
ecletica-56	212	7	table	table	NOUN
ecletica-56	212	8	1	1	NUM
ecletica-56	212	9	were	be	AUX
ecletica-56	212	10	statistically	statistically	ADV
ecletica-56	212	11	analyzed	analyze	VERB
ecletica-56	212	12	using	use	VERB
ecletica-56	212	13	the	the	DET
ecletica-56	212	14	paired	pair	VERB
ecletica-56	212	15	student	student	NOUN
ecletica-56	212	16	’s	’s	PART
ecletica-56	212	17	t	t	PROPN
ecletica-56	212	18	test	test	NOUN
ecletica-56	212	19	and	and	CCONJ
ecletica-56	212	20	the	the	DET
ecletica-56	212	21	snedecor	snedecor	NOUN
ecletica-56	212	22	f	f	PROPN
ecletica-56	212	23	test	test	NOUN
ecletica-56	213	1	[	[	X
ecletica-56	213	2	36	36	NUM
ecletica-56	213	3	]	]	X
ecletica-56	213	4	(	(	PUNCT
ecletica-56	213	5	table	table	NOUN
ecletica-56	213	6	2	2	NUM
ecletica-56	213	7	)	)	PUNCT
ecletica-56	213	8	.	.	PUNCT
ecletica-56	214	1	table	table	NOUN
ecletica-56	214	2	2	2	NUM
ecletica-56	214	3	.	.	PUNCT
ecletica-56	214	4	comparison	comparison	NOUN
ecletica-56	214	5	of	of	ADP
ecletica-56	214	6	the	the	DET
ecletica-56	214	7	analytical	analytical	ADJ
ecletica-56	214	8	results	result	NOUN
ecletica-56	214	9	using	use	VERB
ecletica-56	214	10	the	the	DET
ecletica-56	214	11	student	student	NOUN
ecletica-56	214	12	’s	’s	PART
ecletica-56	214	13	paired	pair	VERB
ecletica-56	214	14	t	t	PROPN
ecletica-56	214	15	test	test	NOUN
ecletica-56	214	16	and	and	CCONJ
ecletica-56	214	17	the	the	DET
ecletica-56	214	18	snedecor	snedecor	NOUN
ecletica-56	214	19	f	f	PROPN
ecletica-56	214	20	test	test	NOUN
ecletica-56	215	1	[	[	X
ecletica-56	215	2	36	36	NUM
ecletica-56	215	3	]	]	PUNCT
ecletica-56	215	4	.	.	PUNCT
ecletica-56	216	1	methods	method	NOUN
ecletica-56	216	2	compared	compare	VERB
ecletica-56	216	3	t	t	PROPN
ecletica-56	216	4	calc	calc	PROPN
ecletica-56	216	5	f	f	PROPN
ecletica-56	216	6	calc	calc	PROPN
ecletica-56	217	1	i	i	PROPN
ecletica-56	217	2	ii	ii	VERB
ecletica-56	218	1	i	i	PRON
ecletica-56	218	2	ii	ii	NOUN
ecletica-56	218	3	grav	grav	PROPN
ecletica-56	218	4	t	t	PROPN
ecletica-56	218	5	vs.	vs.	ADP
ecletica-56	218	6	grav	grav	PROPN
ecletica-56	218	7	f	f	PROPN
ecletica-56	218	8	0.1	0.1	NUM
ecletica-56	218	9	0.4	0.4	NUM
ecletica-56	218	10	19.5	19.5	NUM
ecletica-56	218	11	14.1	14.1	NUM
ecletica-56	218	12	grav	grav	NOUN
ecletica-56	218	13	t	t	PROPN
ecletica-56	218	14	vs.	vs.	ADP
ecletica-56	218	15	official	official	NOUN
ecletica-56	218	16	(	(	PUNCT
ecletica-56	218	17	pot	pot	NOUN
ecletica-56	218	18	.	.	PUNCT
ecletica-56	218	19	)	)	PUNCT
ecletica-56	219	1	2.7	2.7	NUM
ecletica-56	219	2	2.7	2.7	NUM
ecletica-56	219	3	10.5	10.5	NUM
ecletica-56	219	4	3.5	3.5	NUM
ecletica-56	219	5	grav	grav	NOUN
ecletica-56	219	6	f	f	PROPN
ecletica-56	219	7	vs.	vs.	ADP
ecletica-56	219	8	official	official	NOUN
ecletica-56	219	9	(	(	PUNCT
ecletica-56	219	10	pot	pot	NOUN
ecletica-56	219	11	.	.	PUNCT
ecletica-56	219	12	)	)	PUNCT
ecletica-56	220	1	1.6	1.6	NUM
ecletica-56	220	2	1.0	1.0	NUM
ecletica-56	220	3	1.9	1.9	NUM
ecletica-56	220	4	4.0	4.0	NUM
ecletica-56	220	5	grav	grav	NOUN
ecletica-56	220	6	t	t	PROPN
ecletica-56	220	7	vs.	vs.	ADP
ecletica-56	220	8	hplc	hplc	PROPN
ecletica-56	220	9	2.7	2.7	NUM
ecletica-56	220	10	8.0	8.0	NUM
ecletica-56	220	11	78.9	78.9	NUM
ecletica-56	220	12	1.5	1.5	NUM
ecletica-56	220	13	grav	grav	NOUN
ecletica-56	220	14	f	f	PROPN
ecletica-56	220	15	vs.	vs.	ADP
ecletica-56	220	16	hplc	hplc	PROPN
ecletica-56	220	17	2.4	2.4	NUM
ecletica-56	220	18	2.8	2.8	NUM
ecletica-56	220	19	4.1	4.1	NUM
ecletica-56	220	20	9.6	9.6	NUM
ecletica-56	220	21	hplc	hplc	NOUN
ecletica-56	220	22	vs.	vs.	ADP
ecletica-56	220	23	official	official	NOUN
ecletica-56	220	24	(	(	PUNCT
ecletica-56	220	25	pot	pot	NOUN
ecletica-56	220	26	.	.	PUNCT
ecletica-56	220	27	)	)	PUNCT
ecletica-56	221	1	1.6	1.6	NUM
ecletica-56	221	2	3.1	3.1	NUM
ecletica-56	221	3	7.5	7.5	NUM
ecletica-56	221	4	2.4	2.4	NUM
ecletica-56	221	5			NOUN
ecletica-56	221	6	=	=	PUNCT
ecletica-56	221	7	(	(	PUNCT
ecletica-56	221	8	na	na	PART
ecletica-56	221	9	+	+	NUM
ecletica-56	221	10	nb	nb	INTJ
ecletica-56	221	11	–	–	PUNCT
ecletica-56	221	12	2	2	NUM
ecletica-56	221	13	)	)	PUNCT
ecletica-56	221	14	=	=	SYM
ecletica-56	221	15	4	4	NUM
ecletica-56	221	16	;	;	PUNCT
ecletica-56	221	17	at	at	ADP
ecletica-56	221	18	the	the	DET
ecletica-56	221	19	95	95	NUM
ecletica-56	221	20	%	%	NOUN
ecletica-56	221	21	confidence	confidence	NOUN
ecletica-56	221	22	level	level	NOUN
ecletica-56	221	23	.	.	PUNCT
ecletica-56	222	1	ttab=2.8	ttab=2.8	NOUN
ecletica-56	222	2	and	and	CCONJ
ecletica-56	222	3	ftab=19.0	ftab=19.0	ADJ
ecletica-56	222	4	;	;	PUNCT
ecletica-56	222	5	at	at	ADP
ecletica-56	222	6	the	the	DET
ecletica-56	222	7	99	99	NUM
ecletica-56	222	8	%	%	NOUN
ecletica-56	222	9	confidence	confidence	NOUN
ecletica-56	222	10	level	level	NOUN
ecletica-56	222	11	ttab=	ttab=	NUM
ecletica-56	222	12	4.604	4.604	NUM
ecletica-56	222	13	and	and	CCONJ
ecletica-56	222	14	ftab=99.0	ftab=99.0	ADJ
ecletica-56	222	15	grav	grav	PROPN
ecletica-56	222	16	.	.	PUNCT
ecletica-56	223	1	t	t	PROPN
ecletica-56	223	2	=	=	PUNCT
ecletica-56	223	3	proposed	propose	VERB
ecletica-56	223	4	gravimetric	gravimetric	NOUN
ecletica-56	223	5	;	;	PUNCT
ecletica-56	223	6	filtration	filtration	NOUN
ecletica-56	223	7	using	use	VERB
ecletica-56	223	8	glass	glass	NOUN
ecletica-56	223	9	tubes	tube	NOUN
ecletica-56	223	10	with	with	ADP
ecletica-56	223	11	sintered	sinter	VERB
ecletica-56	223	12	disc	disc	NOUN
ecletica-56	223	13	.	.	PUNCT
ecletica-56	224	1	grav	grav	PROPN
ecletica-56	224	2	.	.	PUNCT
ecletica-56	225	1	f	f	PROPN
ecletica-56	226	1	=	=	PRON
ecletica-56	226	2	proposed	propose	VERB
ecletica-56	226	3	gravimetric	gravimetric	NOUN
ecletica-56	226	4	;	;	PUNCT
ecletica-56	226	5	filtration	filtration	NOUN
ecletica-56	226	6	using	use	VERB
ecletica-56	226	7	syringe	syringe	NOUN
ecletica-56	226	8	filters	filter	NOUN
ecletica-56	226	9	.	.	PUNCT
ecletica-56	227	1	hplc	hplc	NOUN
ecletica-56	227	2	=	=	SYM
ecletica-56	227	3	high	high	ADJ
ecletica-56	227	4	pressure	pressure	NOUN
ecletica-56	227	5	liquid	liquid	NOUN
ecletica-56	227	6	chromatography	chromatography	NOUN
ecletica-56	227	7	.	.	PUNCT
ecletica-56	228	1	official	official	ADJ
ecletica-56	228	2	method	method	NOUN
ecletica-56	228	3	:	:	PUNCT
ecletica-56	228	4	potentiometric	potentiometric	ADJ
ecletica-56	228	5	titration	titration	NOUN
ecletica-56	228	6	.	.	PUNCT
ecletica-56	229	1	it	it	PRON
ecletica-56	229	2	can	can	AUX
ecletica-56	229	3	be	be	AUX
ecletica-56	229	4	observed	observe	VERB
ecletica-56	229	5	that	that	SCONJ
ecletica-56	229	6	the	the	DET
ecletica-56	229	7	calculated	calculated	ADJ
ecletica-56	229	8	t	t	PROPN
ecletica-56	229	9	and	and	CCONJ
ecletica-56	229	10	f	f	PROPN
ecletica-56	229	11	values	value	NOUN
ecletica-56	229	12	are	be	AUX
ecletica-56	229	13	smaller	small	ADJ
ecletica-56	229	14	than	than	ADP
ecletica-56	229	15	those	those	PRON
ecletica-56	229	16	tabulated	tabulate	VERB
ecletica-56	229	17	,	,	PUNCT
ecletica-56	229	18	when	when	SCONJ
ecletica-56	229	19	the	the	DET
ecletica-56	229	20	proposed	propose	VERB
ecletica-56	229	21	gravimetric	gravimetric	ADJ
ecletica-56	229	22	procedures	procedure	NOUN
ecletica-56	229	23	are	be	AUX
ecletica-56	229	24	compared	compare	VERB
ecletica-56	229	25	with	with	ADP
ecletica-56	229	26	the	the	DET
ecletica-56	229	27	potenciometric	potenciometric	ADJ
ecletica-56	229	28	official	official	ADJ
ecletica-56	229	29	method	method	NOUN
ecletica-56	229	30	,	,	PUNCT
ecletica-56	229	31	indicating	indicate	VERB
ecletica-56	229	32	equivalent	equivalent	ADJ
ecletica-56	229	33	results	result	NOUN
ecletica-56	229	34	and	and	CCONJ
ecletica-56	229	35	precision	precision	NOUN
ecletica-56	229	36	.	.	PUNCT
ecletica-56	230	1	in	in	ADP
ecletica-56	230	2	the	the	DET
ecletica-56	230	3	hplc	hplc	NOUN
ecletica-56	230	4	cases	case	VERB
ecletica-56	230	5	two	two	NUM
ecletica-56	230	6	small	small	ADJ
ecletica-56	230	7	differences	difference	NOUN
ecletica-56	230	8	are	be	AUX
ecletica-56	230	9	observed	observe	VERB
ecletica-56	230	10	in	in	ADP
ecletica-56	230	11	t	t	NOUN
ecletica-56	230	12	values	value	NOUN
ecletica-56	230	13	and	and	CCONJ
ecletica-56	230	14	one	one	NUM
ecletica-56	230	15	in	in	ADP
ecletica-56	230	16	f	f	PROPN
ecletica-56	230	17	values	value	NOUN
ecletica-56	230	18	when	when	SCONJ
ecletica-56	230	19	comparison	comparison	NOUN
ecletica-56	230	20	is	be	AUX
ecletica-56	230	21	done	do	VERB
ecletica-56	230	22	with	with	ADP
ecletica-56	230	23	the	the	DET
ecletica-56	230	24	gravimetric	gravimetric	ADJ
ecletica-56	230	25	method	method	NOUN
ecletica-56	230	26	where	where	SCONJ
ecletica-56	230	27	a	a	DET
ecletica-56	230	28	glass	glass	NOUN
ecletica-56	230	29	tube	tube	NOUN
ecletica-56	230	30	with	with	ADP
ecletica-56	230	31	sintered	sinter	VERB
ecletica-56	230	32	disc	disc	NOUN
ecletica-56	230	33	is	be	AUX
ecletica-56	230	34	used	use	VERB
ecletica-56	230	35	and	and	CCONJ
ecletica-56	230	36	with	with	ADP
ecletica-56	230	37	the	the	DET
ecletica-56	230	38	official	official	ADJ
ecletica-56	230	39	titrimetric	titrimetric	ADJ
ecletica-56	230	40	procedure	procedure	NOUN
ecletica-56	230	41	.	.	PUNCT
ecletica-56	231	1	however	however	ADV
ecletica-56	231	2	,	,	PUNCT
ecletica-56	231	3	if	if	SCONJ
ecletica-56	231	4	the	the	DET
ecletica-56	231	5	99	99	NUM
ecletica-56	231	6	%	%	NOUN
ecletica-56	231	7	confidence	confidence	NOUN
ecletica-56	231	8	level	level	NOUN
ecletica-56	231	9	is	be	AUX
ecletica-56	231	10	considered	consider	VERB
ecletica-56	231	11	all	all	DET
ecletica-56	231	12	results	result	NOUN
ecletica-56	231	13	become	become	VERB
ecletica-56	231	14	is	be	AUX
ecletica-56	231	15	agreement	agreement	NOUN
ecletica-56	231	16	.	.	PUNCT
ecletica-56	232	1	conclusion	conclusion	NOUN
ecletica-56	232	2	the	the	DET
ecletica-56	232	3	proposed	propose	VERB
ecletica-56	232	4	method	method	NOUN
ecletica-56	232	5	presents	present	VERB
ecletica-56	232	6	some	some	DET
ecletica-56	232	7	interesting	interesting	ADJ
ecletica-56	232	8	characteristics	characteristic	NOUN
ecletica-56	232	9	.	.	PUNCT
ecletica-56	233	1	it	it	PRON
ecletica-56	233	2	easy	easy	ADJ
ecletica-56	233	3	and	and	CCONJ
ecletica-56	233	4	relatively	relatively	ADV
ecletica-56	233	5	fast	fast	ADJ
ecletica-56	233	6	to	to	PART
ecletica-56	233	7	be	be	AUX
ecletica-56	233	8	performed	perform	VERB
ecletica-56	233	9	;	;	PUNCT
ecletica-56	233	10	it	it	PRON
ecletica-56	233	11	is	be	AUX
ecletica-56	233	12	very	very	ADV
ecletica-56	233	13	reliable	reliable	ADJ
ecletica-56	233	14	and	and	CCONJ
ecletica-56	233	15	inexpensive	inexpensive	ADJ
ecletica-56	233	16	;	;	PUNCT
ecletica-56	233	17	a	a	DET
ecletica-56	233	18	calibration	calibration	NOUN
ecletica-56	233	19	plot	plot	NOUN
ecletica-56	233	20	is	be	AUX
ecletica-56	233	21	unnecessary	unnecessary	ADJ
ecletica-56	233	22	because	because	SCONJ
ecletica-56	233	23	it	it	PRON
ecletica-56	233	24	is	be	AUX
ecletica-56	233	25	an	an	DET
ecletica-56	233	26	absolute	absolute	ADJ
ecletica-56	233	27	method	method	NOUN
ecletica-56	233	28	;	;	PUNCT
ecletica-56	233	29	it	it	PRON
ecletica-56	233	30	is	be	AUX
ecletica-56	233	31	a	a	DET
ecletica-56	233	32	green	green	ADJ
ecletica-56	233	33	procedure	procedure	NOUN
ecletica-56	233	34	as	as	SCONJ
ecletica-56	233	35	does	do	AUX
ecletica-56	233	36	not	not	PART
ecletica-56	233	37	uses	use	VERB
ecletica-56	233	38	organic	organic	ADJ
ecletica-56	233	39	or	or	CCONJ
ecletica-56	233	40	solvents	solvent	NOUN
ecletica-56	233	41	or	or	CCONJ
ecletica-56	233	42	toxic	toxic	ADJ
ecletica-56	233	43	substances	substance	NOUN
ecletica-56	233	44	(	(	PUNCT
ecletica-56	233	45	excepting	except	VERB
ecletica-56	233	46	small	small	ADJ
ecletica-56	233	47	quantities	quantity	NOUN
ecletica-56	233	48	of	of	ADP
ecletica-56	233	49	ammonia	ammonia	NOUN
ecletica-56	233	50	)	)	PUNCT
ecletica-56	233	51	and	and	CCONJ
ecletica-56	233	52	those	those	PRON
ecletica-56	233	53	used	use	VERB
ecletica-56	233	54	are	be	AUX
ecletica-56	233	55	in	in	ADP
ecletica-56	233	56	small	small	ADJ
ecletica-56	233	57	quantities	quantity	NOUN
ecletica-56	233	58	.	.	PUNCT
ecletica-56	234	1	therefore	therefore	ADV
ecletica-56	234	2	the	the	DET
ecletica-56	234	3	proposed	propose	VERB
ecletica-56	234	4	method	method	NOUN
ecletica-56	234	5	can	can	AUX
ecletica-56	234	6	be	be	AUX
ecletica-56	234	7	suggested	suggest	VERB
ecletica-56	234	8	for	for	ADP
ecletica-56	234	9	the	the	DET
ecletica-56	234	10	analysis	analysis	NOUN
ecletica-56	234	11	of	of	ADP
ecletica-56	234	12	metformin	metformin	NOUN
ecletica-56	234	13	in	in	ADP
ecletica-56	234	14	the	the	DET
ecletica-56	234	15	bulk	bulk	ADJ
ecletica-56	234	16	drug	drug	NOUN
ecletica-56	234	17	and	and	CCONJ
ecletica-56	234	18	in	in	ADP
ecletica-56	234	19	pharmaceutical	pharmaceutical	ADJ
ecletica-56	234	20	preparations	preparation	NOUN
ecletica-56	234	21	.	.	PUNCT
ecletica-56	235	1	acknowledgments	acknowledgment	NOUN
ecletica-56	235	2	the	the	DET
ecletica-56	235	3	authors	author	NOUN
ecletica-56	235	4	are	be	AUX
ecletica-56	235	5	grateful	grateful	ADJ
ecletica-56	235	6	to	to	PART
ecletica-56	235	7	cnpq	cnpq	NOUN
ecletica-56	235	8	,	,	PUNCT
ecletica-56	235	9	fapesp	fapesp	NOUN
ecletica-56	235	10	and	and	CCONJ
ecletica-56	235	11	capes	cape	NOUN
ecletica-56	235	12	for	for	ADP
ecletica-56	235	13	financial	financial	ADJ
ecletica-56	235	14	support	support	NOUN
ecletica-56	235	15	and	and	CCONJ
ecletica-56	235	16	to	to	PART
ecletica-56	235	17	prof	prof	PROPN
ecletica-56	235	18	.	.	PUNCT
ecletica-56	236	1	dr	dr	PROPN
ecletica-56	236	2	.	.	PROPN
ecletica-56	236	3	carol	carol	PROPN
ecletica-56	236	4	h.	h.	PROPN
ecletica-56	236	5	collins	collins	PROPN
ecletica-56	236	6	for	for	ADP
ecletica-56	236	7	english	english	ADJ
ecletica-56	236	8	revision	revision	NOUN
ecletica-56	236	9	of	of	ADP
ecletica-56	236	10	the	the	DET
ecletica-56	236	11	manuscript	manuscript	NOUN
ecletica-56	236	12	.	.	PUNCT
ecletica-56	237	1	referências	referências	PROPN
ecletica-56	237	2	[	[	X
ecletica-56	237	3	1	1	X
ecletica-56	237	4	]	]	X
ecletica-56	237	5	m.c	m.c	PROPN
ecletica-56	237	6	.	.	PROPN
ecletica-56	237	7	foss	foss	PROPN
ecletica-56	237	8	,	,	PUNCT
ecletica-56	237	9	diabetes	diabete	VERB
ecletica-56	237	10	mellitus	mellitus	NOUN
ecletica-56	237	11	:	:	PUNCT
ecletica-56	238	1	conceito	conceito	PROPN
ecletica-56	238	2	,	,	PUNCT
ecletica-56	238	3	diagnóstico	diagnóstico	PROPN
ecletica-56	238	4	e	e	PROPN
ecletica-56	238	5	classificação	classificação	PROPN
ecletica-56	238	6	,	,	PUNCT
ecletica-56	238	7	rev	rev	PROPN
ecletica-56	238	8	.	.	PROPN
ecletica-56	238	9	med	med	PROPN
ecletica-56	238	10	.	.	PROPN
ecletica-56	238	11	ribeirão	ribeirão	PROPN
ecletica-56	238	12	preto	preto	VERB
ecletica-56	238	13	22	22	NUM
ecletica-56	238	14	(	(	PUNCT
ecletica-56	238	15	1989	1989	NUM
ecletica-56	238	16	)	)	PUNCT
ecletica-56	238	17	,	,	PUNCT
ecletica-56	238	18	54	54	NUM
ecletica-56	238	19	-	-	SYM
ecletica-56	238	20	61	61	NUM
ecletica-56	238	21	.	.	PUNCT
ecletica-56	239	1	eclética	eclética	PROPN
ecletica-56	239	2	química	química	PROPN
ecletica-56	239	3	,	,	PUNCT
ecletica-56	239	4	vol	vol	NOUN
ecletica-56	239	5	.	.	PROPN
ecletica-56	239	6	40	40	NUM
ecletica-56	239	7	,	,	PUNCT
ecletica-56	239	8	62	62	NUM
ecletica-56	239	9	-	-	SYM
ecletica-56	239	10	70	70	NUM
ecletica-56	239	11	,	,	PUNCT
ecletica-56	239	12	2015	2015	NUM
ecletica-56	239	13	.	.	PUNCT
ecletica-56	240	1	68	68	NUM
ecletica-56	240	2	68	68	NUM
ecletica-56	240	3	[	[	X
ecletica-56	240	4	2	2	NUM
ecletica-56	240	5	]	]	PUNCT
ecletica-56	240	6	m.t.c.g	m.t.c.g	PROPN
ecletica-56	240	7	torquato	torquato	PROPN
ecletica-56	240	8	,	,	PUNCT
ecletica-56	240	9	r.m	r.m	PROPN
ecletica-56	240	10	.	.	PROPN
ecletica-56	240	11	montenegro	montenegro	PROPN
ecletica-56	240	12	junior	junior	PROPN
ecletica-56	240	13	,	,	PUNCT
ecletica-56	240	14	l.a.l	l.a.l	PROPN
ecletica-56	240	15	viana	viana	PROPN
ecletica-56	240	16	,	,	PUNCT
ecletica-56	240	17	r.a.h.g	r.a.h.g	PROPN
ecletica-56	240	18	.	.	PROPN
ecletica-56	240	19	souza	souza	PROPN
ecletica-56	240	20	,	,	PUNCT
ecletica-56	240	21	m.m	m.m	PROPN
ecletica-56	240	22	.	.	PROPN
ecletica-56	240	23	lanna	lanna	PROPN
ecletica-56	240	24	,	,	PUNCT
ecletica-56	240	25	j.c.b	j.c.b	PROPN
ecletica-56	240	26	luca	luca	PROPN
ecletica-56	240	27	,	,	PUNCT
ecletica-56	240	28	c.	c.	PROPN
ecletica-56	240	29	bidurin	bidurin	PROPN
ecletica-56	240	30	,	,	PUNCT
ecletica-56	240	31	m.c	m.c	PROPN
ecletica-56	240	32	.	.	PROPN
ecletica-56	240	33	foss	foss	PROPN
ecletica-56	240	34	,	,	PUNCT
ecletica-56	240	35	prevalence	prevalence	NOUN
ecletica-56	240	36	of	of	ADP
ecletica-56	240	37	diabetes	diabetes	NOUN
ecletica-56	240	38	mellitus	mellitus	NOUN
ecletica-56	240	39	and	and	CCONJ
ecletica-56	240	40	impaired	impaired	ADJ
ecletica-56	240	41	glucose	glucose	NOUN
ecletica-56	240	42	tolerance	tolerance	NOUN
ecletica-56	240	43	in	in	ADP
ecletica-56	240	44	the	the	DET
ecletica-56	240	45	urban	urban	ADJ
ecletica-56	240	46	population	population	NOUN
ecletica-56	240	47	aged	age	VERB
ecletica-56	240	48	30	30	NUM
ecletica-56	240	49	-	-	SYM
ecletica-56	240	50	69	69	NUM
ecletica-56	240	51	years	year	NOUN
ecletica-56	240	52	in	in	ADP
ecletica-56	240	53	ribeirão	ribeirão	PROPN
ecletica-56	240	54	preto	preto	PROPN
ecletica-56	240	55	(	(	PUNCT
ecletica-56	240	56	são	são	PROPN
ecletica-56	240	57	paulo	paulo	PROPN
ecletica-56	240	58	)	)	PUNCT
ecletica-56	240	59	,	,	PUNCT
ecletica-56	240	60	brazil	brazil	PROPN
ecletica-56	240	61	,	,	PUNCT
ecletica-56	240	62	são	são	PROPN
ecletica-56	240	63	paulo	paulo	PROPN
ecletica-56	240	64	med	med	PROPN
ecletica-56	240	65	.	.	PUNCT
ecletica-56	241	1	j.121(2006	j.121(2006	PROPN
ecletica-56	241	2	)	)	PUNCT
ecletica-56	241	3	224	224	NUM
ecletica-56	241	4	-	-	SYM
ecletica-56	241	5	230	230	NUM
ecletica-56	241	6	.	.	PUNCT
ecletica-56	242	1	[	[	X
ecletica-56	242	2	3	3	X
ecletica-56	242	3	]	]	X
ecletica-56	242	4	m.o	m.o	PROPN
ecletica-56	242	5	.	.	PROPN
ecletica-56	242	6	goodarzi	goodarzi	PROPN
ecletica-56	242	7	,	,	PUNCT
ecletica-56	242	8	m.	m.	NOUN
ecletica-56	242	9	bryer	bryer	PROPN
ecletica-56	242	10	-	-	PUNCT
ecletica-56	242	11	ash	ash	NOUN
ecletica-56	242	12	,	,	PUNCT
ecletica-56	242	13	metformin	metformin	NOUN
ecletica-56	242	14	revisited	revisit	VERB
ecletica-56	242	15	:	:	PUNCT
ecletica-56	242	16	re	re	NOUN
ecletica-56	242	17	-	-	NOUN
ecletica-56	242	18	evaluation	evaluation	NOUN
ecletica-56	242	19	of	of	ADP
ecletica-56	242	20	its	its	PRON
ecletica-56	242	21	properties	property	NOUN
ecletica-56	242	22	and	and	CCONJ
ecletica-56	242	23	role	role	NOUN
ecletica-56	242	24	in	in	ADP
ecletica-56	242	25	the	the	DET
ecletica-56	242	26	pharmacopoeia	pharmacopoeia	NOUN
ecletica-56	242	27	of	of	ADP
ecletica-56	242	28	modern	modern	ADJ
ecletica-56	242	29	antidiabetic	antidiabetic	ADJ
ecletica-56	242	30	agents	agent	NOUN
ecletica-56	242	31	.	.	PUNCT
ecletica-56	243	1	diabetes	diabetes	NOUN
ecletica-56	243	2	obes	obe	NOUN
ecletica-56	243	3	.	.	PUNCT
ecletica-56	244	1	metabolism	metabolism	NOUN
ecletica-56	244	2	,	,	PUNCT
ecletica-56	244	3	7(2005	7(2005	X
ecletica-56	244	4	)	)	PUNCT
ecletica-56	244	5	654	654	NUM
ecletica-56	244	6	-	-	SYM
ecletica-56	244	7	665	665	NUM
ecletica-56	244	8	.	.	PUNCT
ecletica-56	245	1	[	[	X
ecletica-56	245	2	4	4	X
ecletica-56	245	3	]	]	X
ecletica-56	245	4	e.	e.	PROPN
ecletica-56	245	5	reynolds	reynolds	PROPN
ecletica-56	245	6	(	(	PUNCT
ecletica-56	245	7	eds	ed	NOUN
ecletica-56	245	8	)	)	PUNCT
ecletica-56	245	9	,	,	PUNCT
ecletica-56	245	10	martindale	martindale	PROPN
ecletica-56	245	11	:	:	PUNCT
ecletica-56	245	12	the	the	DET
ecletica-56	245	13	extra	extra	ADJ
ecletica-56	245	14	pharmacopoeia	pharmacopoeia	NOUN
ecletica-56	245	15	,	,	PUNCT
ecletica-56	245	16	twenty	twenty	NUM
ecletica-56	245	17	-	-	PUNCT
ecletica-56	245	18	ninth	ninth	ADJ
ecletica-56	245	19	ed	ed	NOUN
ecletica-56	245	20	.	.	PROPN
ecletica-56	245	21	,	,	PUNCT
ecletica-56	245	22	the	the	DET
ecletica-56	245	23	pharmaceutical	pharmaceutical	NOUN
ecletica-56	245	24	press	press	NOUN
ecletica-56	245	25	,	,	PUNCT
ecletica-56	245	26	london	london	PROPN
ecletica-56	245	27	,	,	PUNCT
ecletica-56	245	28	1989	1989	NUM
ecletica-56	245	29	[	[	X
ecletica-56	245	30	5	5	NUM
ecletica-56	245	31	]	]	PUNCT
ecletica-56	245	32	a.	a.	NOUN
ecletica-56	245	33	kleemann	kleemann	PROPN
ecletica-56	245	34	,	,	PUNCT
ecletica-56	245	35	j.	j.	PROPN
ecletica-56	245	36	engel	engel	PROPN
ecletica-56	245	37	,	,	PUNCT
ecletica-56	245	38	b.	b.	PROPN
ecletica-56	245	39	kutscher	kutscher	PROPN
ecletica-56	245	40	,	,	PUNCT
ecletica-56	245	41	d.	d.	PROPN
ecletica-56	245	42	reichert	reichert	PROPN
ecletica-56	245	43	,	,	PUNCT
ecletica-56	245	44	pharmaceutical	pharmaceutical	ADJ
ecletica-56	245	45	substances	substance	NOUN
ecletica-56	245	46	:	:	PUNCT
ecletica-56	245	47	syntesis	syntesis	NOUN
ecletica-56	245	48	,	,	PUNCT
ecletica-56	245	49	pattens	patten	NOUN
ecletica-56	245	50	,	,	PUNCT
ecletica-56	245	51	applications	application	NOUN
ecletica-56	245	52	,	,	PUNCT
ecletica-56	245	53	v.	v.	ADP
ecletica-56	245	54	1	1	NUM
ecletica-56	245	55	(	(	PUNCT
ecletica-56	245	56	a	a	DET
ecletica-56	245	57	-	-	PUNCT
ecletica-56	245	58	m	m	NOUN
ecletica-56	245	59	)	)	PUNCT
ecletica-56	245	60	,	,	PUNCT
ecletica-56	245	61	fourth	fourth	ADJ
ecletica-56	245	62	ed	ed	NOUN
ecletica-56	245	63	.	.	PROPN
ecletica-56	245	64	,	,	PUNCT
ecletica-56	245	65	thieme	thieme	PROPN
ecletica-56	245	66	,	,	PUNCT
ecletica-56	245	67	stuttgart	stuttgart	PROPN
ecletica-56	245	68	,	,	PUNCT
ecletica-56	245	69	2001	2001	NUM
ecletica-56	245	70	[	[	X
ecletica-56	245	71	6	6	NUM
ecletica-56	245	72	]	]	PUNCT
ecletica-56	245	73	m.	m.	PROPN
ecletica-56	245	74	b.	b.	PROPN
ecletica-56	245	75	gomes	gomes	PROPN
ecletica-56	245	76	,	,	PUNCT
ecletica-56	245	77	s.	s.	PROPN
ecletica-56	245	78	cailleaux	cailleaux	PROPN
ecletica-56	245	79	,	,	PUNCT
ecletica-56	245	80	e.	e.	PROPN
ecletica-56	245	81	tibiriçá	tibiriçá	PROPN
ecletica-56	245	82	,	,	PUNCT
ecletica-56	245	83	efeitos	efeitos	ADJ
ecletica-56	245	84	da	da	PROPN
ecletica-56	245	85	metformina	metformina	NOUN
ecletica-56	245	86	na	na	PART
ecletica-56	245	87	disfunção	disfunção	VERB
ecletica-56	245	88	endotelial	endotelial	ADJ
ecletica-56	245	89	da	da	PROPN
ecletica-56	245	90	circulação	circulação	PROPN
ecletica-56	245	91	renal	renal	PROPN
ecletica-56	245	92	induzida	induzida	PROPN
ecletica-56	245	93	pela	pela	PROPN
ecletica-56	245	94	hiperglicemia	hiperglicemia	INTJ
ecletica-56	246	1	em	em	PRON
ecletica-56	246	2	coelhos	coelhos	PROPN
ecletica-56	246	3	não	não	PROPN
ecletica-56	246	4	diabéticos	diabéticos	PROPN
ecletica-56	246	5	,	,	PUNCT
ecletica-56	246	6	arq	arq	PROPN
ecletica-56	246	7	.	.	PUNCT
ecletica-56	246	8	bras	bras	PROPN
ecletica-56	246	9	.	.	PUNCT
ecletica-56	247	1	endocrinol	endocrinol	NOUN
ecletica-56	247	2	.	.	PUNCT
ecletica-56	248	1	metab	metab	PROPN
ecletica-56	248	2	.	.	PUNCT
ecletica-56	249	1	49	49	NUM
ecletica-56	249	2	(	(	PUNCT
ecletica-56	249	3	2005	2005	NUM
ecletica-56	249	4	)	)	PUNCT
ecletica-56	249	5	938	938	NUM
ecletica-56	249	6	-	-	SYM
ecletica-56	249	7	943	943	NUM
ecletica-56	249	8	.	.	PUNCT
ecletica-56	250	1	[	[	X
ecletica-56	250	2	7	7	X
ecletica-56	250	3	]	]	X
ecletica-56	250	4	c.	c.	PROPN
ecletica-56	250	5	l.	l.	PROPN
ecletica-56	250	6	li	li	PROPN
ecletica-56	250	7	,	,	PUNCT
ecletica-56	250	8	c.y	c.y	PROPN
ecletica-56	250	9	.	.	PROPN
ecletica-56	250	10	pan	pan	PROPN
ecletica-56	250	11	,	,	PUNCT
ecletica-56	250	12	j.m	j.m	PROPN
ecletica-56	250	13	.	.	PROPN
ecletica-56	250	14	lu	lu	PROPN
ecletica-56	250	15	,	,	PUNCT
ecletica-56	250	16	y.	y.	PROPN
ecletica-56	250	17	zhu	zhu	PROPN
ecletica-56	250	18	,	,	PUNCT
ecletica-56	250	19	j.h.wang	j.h.wang	PROPN
ecletica-56	250	20	,	,	PUNCT
ecletica-56	250	21	x.x	x.x	PROPN
ecletica-56	250	22	.	.	PROPN
ecletica-56	250	23	deng	deng	PROPN
ecletica-56	250	24	,	,	PUNCT
ecletica-56	250	25	f.c	f.c	PROPN
ecletica-56	250	26	.	.	PROPN
ecletica-56	250	27	xia	xia	PROPN
ecletica-56	250	28	,	,	PUNCT
ecletica-56	250	29	h.z	h.z	PROPN
ecletica-56	250	30	.	.	PROPN
ecletica-56	250	31	wang	wang	PROPN
ecletica-56	250	32	,	,	PUNCT
ecletica-56	250	33	h.y	h.y	PROPN
ecletica-56	250	34	.	.	PROPN
ecletica-56	250	35	wang	wang	PROPN
ecletica-56	250	36	,	,	PUNCT
ecletica-56	250	37	effect	effect	NOUN
ecletica-56	250	38	of	of	ADP
ecletica-56	250	39	metformin	metformin	NOUN
ecletica-56	250	40	on	on	ADP
ecletica-56	250	41	patients	patient	NOUN
ecletica-56	250	42	with	with	ADP
ecletica-56	250	43	impaired	impaired	ADJ
ecletica-56	250	44	glucose	glucose	NOUN
ecletica-56	250	45	tolerance	tolerance	NOUN
ecletica-56	250	46	,	,	PUNCT
ecletica-56	250	47	diabet	diabet	NOUN
ecletica-56	250	48	.	.	PUNCT
ecletica-56	251	1	med	med	PROPN
ecletica-56	251	2	.	.	PUNCT
ecletica-56	252	1	16	16	NUM
ecletica-56	252	2	(	(	PUNCT
ecletica-56	252	3	1999	1999	NUM
ecletica-56	252	4	)	)	PUNCT
ecletica-56	252	5	477	477	NUM
ecletica-56	252	6	-	-	SYM
ecletica-56	252	7	481	481	NUM
ecletica-56	252	8	.	.	PUNCT
ecletica-56	253	1	[	[	X
ecletica-56	253	2	8	8	NUM
ecletica-56	253	3	]	]	SYM
ecletica-56	253	4	usp	usp	PROPN
ecletica-56	253	5	,	,	PUNCT
ecletica-56	253	6	the	the	DET
ecletica-56	253	7	united	united	PROPN
ecletica-56	253	8	states	states	PROPN
ecletica-56	253	9	pharmacopoeia	pharmacopoeia	PROPN
ecletica-56	253	10	.	.	PUNCT
ecletica-56	254	1	the	the	DET
ecletica-56	254	2	national	national	PROPN
ecletica-56	254	3	formulary	formulary	NOUN
ecletica-56	254	4	,	,	PUNCT
ecletica-56	254	5	thirty	thirty	NUM
ecletica-56	254	6	ed	ed	NOUN
ecletica-56	254	7	.	.	PUNCT
ecletica-56	254	8	,	,	PUNCT
ecletica-56	254	9	nf	nf	PROPN
ecletica-56	254	10	25	25	NUM
ecletica-56	254	11	unites	unite	VERB
ecletica-56	254	12	states	state	VERB
ecletica-56	254	13	pharmacopeial	pharmacopeial	ADJ
ecletica-56	254	14	convention	convention	NOUN
ecletica-56	254	15	,	,	PUNCT
ecletica-56	254	16	rockville	rockville	PROPN
ecletica-56	254	17	,	,	PUNCT
ecletica-56	254	18	2007	2007	NUM
ecletica-56	254	19	,	,	PUNCT
ecletica-56	254	20	pp	pp	ADP
ecletica-56	254	21	2595	2595	NUM
ecletica-56	254	22	-	-	SYM
ecletica-56	254	23	2596	2596	NUM
ecletica-56	254	24	.	.	PUNCT
ecletica-56	255	1	[	[	X
ecletica-56	255	2	9	9	NUM
ecletica-56	255	3	]	]	X
ecletica-56	255	4	japanese	japanese	ADJ
ecletica-56	255	5	pharmacopoeia	pharmacopoeia	NOUN
ecletica-56	255	6	,	,	PUNCT
ecletica-56	255	7	fifteenth	fifteenth	PROPN
ecletica-56	255	8	ed	ed	NOUN
ecletica-56	255	9	.	.	PROPN
ecletica-56	255	10	,	,	PUNCT
ecletica-56	255	11	ministry	ministry	PROPN
ecletica-56	255	12	of	of	ADP
ecletica-56	255	13	healt	healt	PROPN
ecletica-56	255	14	,	,	PUNCT
ecletica-56	255	15	labourand	labourand	NOUN
ecletica-56	255	16	welfare	welfare	NOUN
ecletica-56	255	17	,	,	PUNCT
ecletica-56	255	18	2006	2006	NUM
ecletica-56	255	19	,	,	PUNCT
ecletica-56	255	20	pp	pp	ADP
ecletica-56	255	21	867	867	NUM
ecletica-56	255	22	.	.	PUNCT
ecletica-56	256	1	[	[	X
ecletica-56	256	2	10	10	NUM
ecletica-56	256	3	]	]	X
ecletica-56	256	4	british	british	ADJ
ecletica-56	256	5	pharmacopoeia	pharmacopoeia	NOUN
ecletica-56	256	6	,	,	PUNCT
ecletica-56	256	7	hm	hm	INTJ
ecletica-56	256	8	stationery	stationery	NOUN
ecletica-56	256	9	office	office	NOUN
ecletica-56	256	10	:	:	PUNCT
ecletica-56	256	11	london	london	PROPN
ecletica-56	256	12	,	,	PUNCT
ecletica-56	256	13	1998	1998	NUM
ecletica-56	256	14	,	,	PUNCT
ecletica-56	256	15	p1802	p1802	ADV
ecletica-56	256	16	.	.	PUNCT
ecletica-56	257	1	[	[	X
ecletica-56	257	2	11	11	NUM
ecletica-56	257	3	]	]	X
ecletica-56	257	4	brazilian	brazilian	ADJ
ecletica-56	257	5	pharmacopoeia	pharmacopoeia	NOUN
ecletica-56	257	6	,	,	PUNCT
ecletica-56	257	7	farmacopéia	farmacopéia	ADJ
ecletica-56	257	8	brasileira	brasileira	PROPN
ecletica-56	257	9	,	,	PUNCT
ecletica-56	257	10	organização	organização	PROPN
ecletica-56	257	11	andrei	andrei	PROPN
ecletica-56	257	12	editora	editora	PROPN
ecletica-56	257	13	s.a	s.a	PROPN
ecletica-56	257	14	.	.	PROPN
ecletica-56	257	15	,	,	PUNCT
ecletica-56	257	16	são	são	PROPN
ecletica-56	257	17	paulo	paulo	PROPN
ecletica-56	257	18	,	,	PUNCT
ecletica-56	257	19	1997	1997	NUM
ecletica-56	257	20	,	,	PUNCT
ecletica-56	257	21	pp	pp	ADP
ecletica-56	257	22	1153	1153	NUM
ecletica-56	257	23	.	.	PUNCT
ecletica-56	258	1	[	[	X
ecletica-56	258	2	12	12	NUM
ecletica-56	258	3	]	]	PUNCT
ecletica-56	258	4	m.	m.	PROPN
ecletica-56	258	5	abou	abou	PROPN
ecletica-56	258	6	-	-	PUNCT
ecletica-56	258	7	dan	dan	PROPN
ecletica-56	258	8	,	,	PUNCT
ecletica-56	258	9	s.	s.	PROPN
ecletica-56	258	10	ashour	ashour	PROPN
ecletica-56	258	11	,	,	PUNCT
ecletica-56	258	12	h.	h.	PROPN
ecletica-56	258	13	abou	abou	PROPN
ecletica-56	258	14	-	-	PUNCT
ecletica-56	258	15	dan	dan	PROPN
ecletica-56	258	16	,	,	PUNCT
ecletica-56	258	17	conductometric	conductometric	ADJ
ecletica-56	258	18	titration	titration	NOUN
ecletica-56	258	19	of	of	ADP
ecletica-56	258	20	metformin	metformin	NOUN
ecletica-56	258	21	in	in	ADP
ecletica-56	258	22	pure	pure	ADJ
ecletica-56	258	23	form	form	NOUN
ecletica-56	258	24	and	and	CCONJ
ecletica-56	258	25	in	in	ADP
ecletica-56	258	26	pharmaceutical	pharmaceutical	ADJ
ecletica-56	258	27	preparations	preparation	NOUN
ecletica-56	258	28	using	use	VERB
ecletica-56	258	29	sodiun	sodiun	NOUN
ecletica-56	258	30	tetraphenylborate	tetraphenylborate	NOUN
ecletica-56	258	31	and	and	CCONJ
ecletica-56	258	32	cetylpyridinium	cetylpyridinium	NOUN
ecletica-56	258	33	bromide	bromide	NOUN
ecletica-56	258	34	,	,	PUNCT
ecletica-56	258	35	asian	asian	ADJ
ecletica-56	258	36	j.	j.	PROPN
ecletica-56	258	37	chem	chem	PROPN
ecletica-56	258	38	.	.	PUNCT
ecletica-56	259	1	13	13	NUM
ecletica-56	259	2	(	(	PUNCT
ecletica-56	259	3	2001	2001	NUM
ecletica-56	259	4	)	)	PUNCT
ecletica-56	259	5	1	1	NUM
ecletica-56	259	6	-	-	SYM
ecletica-56	259	7	7	7	NUM
ecletica-56	259	8	.	.	PUNCT
ecletica-56	260	1	[	[	X
ecletica-56	260	2	13	13	NUM
ecletica-56	260	3	]	]	X
ecletica-56	260	4	j.m	j.m	PROPN
ecletica-56	260	5	.	.	PROPN
ecletica-56	260	6	calatayud	calatayud	PROPN
ecletica-56	260	7	,	,	PUNCT
ecletica-56	260	8	p.c	p.c	PROPN
ecletica-56	260	9	.	.	PROPN
ecletica-56	260	10	falcó	falcó	PROPN
ecletica-56	260	11	,	,	PUNCT
ecletica-56	260	12	m.c.p	m.c.p	NOUN
ecletica-56	260	13	.	.	PUNCT
ecletica-56	260	14	marti	marti	PROPN
ecletica-56	260	15	,	,	PUNCT
ecletica-56	260	16	conductimetric	conductimetric	ADJ
ecletica-56	260	17	titration	titration	NOUN
ecletica-56	260	18	of	of	ADP
ecletica-56	260	19	biguanides	biguanide	NOUN
ecletica-56	260	20	,	,	PUNCT
ecletica-56	260	21	copper	copper	NOUN
ecletica-56	260	22	-	-	PUNCT
ecletica-56	260	23	biguanide	biguanide	NOUN
ecletica-56	260	24	complex	complex	ADJ
ecletica-56	260	25	,	,	PUNCT
ecletica-56	260	26	anal	anal	NOUN
ecletica-56	260	27	.	.	PUNCT
ecletica-56	261	1	lett	lett	PROPN
ecletica-56	261	2	.	.	PROPN
ecletica-56	262	1	18	18	NUM
ecletica-56	262	2	(	(	PUNCT
ecletica-56	262	3	1985	1985	NUM
ecletica-56	262	4	)	)	PUNCT
ecletica-56	262	5	1381	1381	NUM
ecletica-56	262	6	-	-	SYM
ecletica-56	262	7	1390	1390	NUM
ecletica-56	262	8	.	.	PUNCT
ecletica-56	263	1	[	[	X
ecletica-56	263	2	14	14	NUM
ecletica-56	263	3	]	]	X
ecletica-56	263	4	e.	e.	PROPN
ecletica-56	263	5	r.	r.	PROPN
ecletica-56	263	6	sartori	sartori	PROPN
ecletica-56	263	7	,	,	PUNCT
ecletica-56	263	8	w.	w.	PROPN
ecletica-56	263	9	t.	t.	PROPN
ecletica-56	263	10	suarez	suarez	PROPN
ecletica-56	263	11	,	,	PUNCT
ecletica-56	263	12	o.	o.	PROPN
ecletica-56	263	13	fatibello	fatibello	PROPN
ecletica-56	263	14	-	-	PUNCT
ecletica-56	263	15	filho	filho	PROPN
ecletica-56	263	16	,	,	PUNCT
ecletica-56	263	17	determinação	determinação	PROPN
ecletica-56	263	18	condutométrica	condutométrica	PROPN
ecletica-56	263	19	de	de	PROPN
ecletica-56	263	20	cloridrato	cloridrato	PROPN
ecletica-56	263	21	de	de	PROPN
ecletica-56	263	22	metformina	metformina	NOUN
ecletica-56	263	23	em	em	PRON
ecletica-56	263	24	formulações	formulações	ADJ
ecletica-56	263	25	farmacêuticas	farmacêutica	NOUN
ecletica-56	263	26	empregando	empregando	ADJ
ecletica-56	263	27	nitrato	nitrato	PROPN
ecletica-56	263	28	de	de	ADP
ecletica-56	263	29	prata	prata	PROPN
ecletica-56	263	30	como	como	PROPN
ecletica-56	263	31	titulante	titulante	PROPN
ecletica-56	263	32	,	,	PUNCT
ecletica-56	263	33	quím	quím	PROPN
ecletica-56	263	34	.	.	PUNCT
ecletica-56	264	1	nova	nova	PROPN
ecletica-56	264	2	32	32	NUM
ecletica-56	264	3	(	(	PUNCT
ecletica-56	264	4	2009	2009	NUM
ecletica-56	264	5	)	)	PUNCT
ecletica-56	264	6	1947	1947	NUM
ecletica-56	264	7	-	-	SYM
ecletica-56	264	8	1950	1950	NUM
ecletica-56	264	9	.	.	PUNCT
ecletica-56	265	1	[	[	X
ecletica-56	265	2	15	15	NUM
ecletica-56	265	3	]	]	X
ecletica-56	265	4	m.m	m.m	PROPN
ecletica-56	265	5	.	.	PROPN
ecletica-56	265	6	annapurna	annapurna	PROPN
ecletica-56	265	7	,	,	PUNCT
ecletica-56	265	8	k.e.v	k.e.v	PROPN
ecletica-56	265	9	.	.	PUNCT
ecletica-56	266	1	nagoji	nagoji	PROPN
ecletica-56	266	2	,	,	PUNCT
ecletica-56	266	3	s.s	s.s	PROPN
ecletica-56	266	4	.	.	PROPN
ecletica-56	266	5	rao	rao	PROPN
ecletica-56	266	6	,	,	PUNCT
ecletica-56	266	7	s.s	s.s	PROPN
ecletica-56	266	8	.	.	PROPN
ecletica-56	266	9	patro	patro	PROPN
ecletica-56	266	10	,	,	PUNCT
ecletica-56	266	11	spectrometric	spectrometric	ADJ
ecletica-56	266	12	estimation	estimation	NOUN
ecletica-56	266	13	of	of	ADP
ecletica-56	266	14	metformin	metformin	NOUN
ecletica-56	266	15	hydrochloride	hydrochloride	NOUN
ecletica-56	266	16	in	in	ADP
ecletica-56	266	17	pharmaceutical	pharmaceutical	ADJ
ecletica-56	266	18	dosage	dosage	NOUN
ecletica-56	266	19	forms	form	NOUN
ecletica-56	266	20	,	,	PUNCT
ecletica-56	266	21	asian	asian	ADJ
ecletica-56	266	22	j.	j.	PROPN
ecletica-56	266	23	chem	chem	PROPN
ecletica-56	266	24	.	.	PUNCT
ecletica-56	267	1	14	14	NUM
ecletica-56	267	2	(	(	PUNCT
ecletica-56	267	3	2002	2002	NUM
ecletica-56	267	4	)	)	PUNCT
ecletica-56	267	5	1775	1775	NUM
ecletica-56	267	6	-	-	SYM
ecletica-56	267	7	1776	1776	NUM
ecletica-56	267	8	.	.	PUNCT
ecletica-56	268	1	[	[	X
ecletica-56	268	2	16	16	NUM
ecletica-56	268	3	]	]	PUNCT
ecletica-56	268	4	s.	s.	PROPN
ecletica-56	268	5	ashour	ashour	PROPN
ecletica-56	268	6	,	,	PUNCT
ecletica-56	268	7	r.	r.	PROPN
ecletica-56	268	8	kabbani	kabbani	PROPN
ecletica-56	268	9	,	,	PUNCT
ecletica-56	268	10	direct	direct	ADJ
ecletica-56	268	11	spectrophotometric	spectrophotometric	ADJ
ecletica-56	268	12	determination	determination	NOUN
ecletica-56	268	13	of	of	ADP
ecletica-56	268	14	metformin	metformin	NOUN
ecletica-56	268	15	hydrochloride	hydrochloride	NOUN
ecletica-56	268	16	in	in	ADP
ecletica-56	268	17	pure	pure	ADJ
ecletica-56	268	18	form	form	NOUN
ecletica-56	268	19	and	and	CCONJ
ecletica-56	268	20	in	in	ADP
ecletica-56	268	21	drug	drug	NOUN
ecletica-56	268	22	formulations	formulation	NOUN
ecletica-56	268	23	,	,	PUNCT
ecletica-56	268	24	anal	anal	NOUN
ecletica-56	268	25	.	.	PUNCT
ecletica-56	269	1	lett	lett	PROPN
ecletica-56	269	2	.	.	PUNCT
ecletica-56	270	1	36	36	NUM
ecletica-56	270	2	(	(	PUNCT
ecletica-56	270	3	2003	2003	NUM
ecletica-56	270	4	)	)	PUNCT
ecletica-56	270	5	361	361	NUM
ecletica-56	270	6	-	-	SYM
ecletica-56	270	7	370	370	NUM
ecletica-56	270	8	.	.	PUNCT
ecletica-56	271	1	[	[	X
ecletica-56	271	2	17	17	NUM
ecletica-56	271	3	]	]	PUNCT
ecletica-56	271	4	s.s.m	s.s.m	NOUN
ecletica-56	271	5	.	.	PUNCT
ecletica-56	272	1	hassan	hassan	PROPN
ecletica-56	272	2	,	,	PUNCT
ecletica-56	272	3	w.h	w.h	PROPN
ecletica-56	272	4	.	.	PROPN
ecletica-56	272	5	mahmoud	mahmoud	PROPN
ecletica-56	272	6	,	,	PUNCT
ecletica-56	272	7	m.a.f	m.a.f	PROPN
ecletica-56	272	8	.	.	PUNCT
ecletica-56	272	9	elmosallamy	elmosallamy	PROPN
ecletica-56	272	10	,	,	PUNCT
ecletica-56	272	11	a.h.m	a.h.m	NOUN
ecletica-56	272	12	.	.	PROPN
ecletica-56	272	13	othman	othman	PROPN
ecletica-56	272	14	,	,	PUNCT
ecletica-56	272	15	determination	determination	NOUN
ecletica-56	272	16	of	of	ADP
ecletica-56	272	17	metformin	metformin	NOUN
ecletica-56	272	18	in	in	ADP
ecletica-56	272	19	pharmaceutical	pharmaceutical	ADJ
ecletica-56	272	20	preparations	preparation	NOUN
ecletica-56	272	21	using	use	VERB
ecletica-56	272	22	potentiometry	potentiometry	NOUN
ecletica-56	272	23	,	,	PUNCT
ecletica-56	272	24	spectrofluorimetry	spectrofluorimetry	NOUN
ecletica-56	272	25	and	and	CCONJ
ecletica-56	272	26	uvvisible	uvvisible	ADJ
ecletica-56	272	27	spectrophometry	spectrophometry	NOUN
ecletica-56	272	28	,	,	PUNCT
ecletica-56	272	29	anal	anal	ADJ
ecletica-56	272	30	.	.	PUNCT
ecletica-56	272	31	chem	chem	PROPN
ecletica-56	272	32	.	.	PUNCT
ecletica-56	273	1	acta	acta	PROPN
ecletica-56	273	2	378	378	NUM
ecletica-56	273	3	(	(	PUNCT
ecletica-56	273	4	1999	1999	NUM
ecletica-56	273	5	)	)	PUNCT
ecletica-56	273	6	299	299	NUM
ecletica-56	273	7	-	-	SYM
ecletica-56	273	8	311	311	NUM
ecletica-56	273	9	.	.	PUNCT
ecletica-56	274	1	[	[	X
ecletica-56	274	2	18	18	NUM
ecletica-56	274	3	]	]	PUNCT
ecletica-56	274	4	m.	m.	NOUN
ecletica-56	274	5	ohta	ohta	PROPN
ecletica-56	274	6	,	,	PUNCT
ecletica-56	274	7	m.	m.	NOUN
ecletica-56	274	8	iwasaki	iwasaki	PROPN
ecletica-56	274	9	,	,	PUNCT
ecletica-56	274	10	m.	m.	NOUN
ecletica-56	274	11	kai	kai	PROPN
ecletica-56	274	12	,	,	PUNCT
ecletica-56	274	13	y.	y.	PROPN
ecletica-56	274	14	ohkura	ohkura	PROPN
ecletica-56	274	15	,	,	PUNCT
ecletica-56	274	16	determination	determination	NOUN
ecletica-56	274	17	of	of	ADP
ecletica-56	274	18	a	a	DET
ecletica-56	274	19	biguanide	biguanide	NOUN
ecletica-56	274	20	metformin	metformin	NOUN
ecletica-56	274	21	by	by	ADP
ecletica-56	274	22	high	high	ADJ
ecletica-56	274	23	-	-	PUNCT
ecletica-56	274	24	performance	performance	NOUN
ecletica-56	274	25	liquid	liquid	ADJ
ecletica-56	274	26	chromatography	chromatography	NOUN
ecletica-56	274	27	with	with	ADP
ecletica-56	274	28	precolumn	precolumn	PROPN
ecletica-56	274	29	fluorescence	fluorescence	NOUN
ecletica-56	274	30	derivatization	derivatization	NOUN
ecletica-56	274	31	,	,	PUNCT
ecletica-56	274	32	anal	anal	NOUN
ecletica-56	274	33	.	.	PUNCT
ecletica-56	275	1	sci	sci	PROPN
ecletica-56	275	2	.	.	PROPN
ecletica-56	275	3	9	9	NUM
ecletica-56	275	4	(	(	PUNCT
ecletica-56	275	5	1993	1993	NUM
ecletica-56	275	6	)	)	PUNCT
ecletica-56	275	7	217	217	NUM
ecletica-56	275	8	-	-	SYM
ecletica-56	275	9	220	220	NUM
ecletica-56	275	10	.	.	PUNCT
ecletica-56	275	11	eclética	eclética	PROPN
ecletica-56	275	12	química	química	PROPN
ecletica-56	275	13	,	,	PUNCT
ecletica-56	275	14	vol	vol	NOUN
ecletica-56	275	15	.	.	PROPN
ecletica-56	275	16	40	40	NUM
ecletica-56	275	17	,	,	PUNCT
ecletica-56	275	18	62	62	NUM
ecletica-56	275	19	-	-	SYM
ecletica-56	275	20	70	70	NUM
ecletica-56	275	21	,	,	PUNCT
ecletica-56	275	22	2015	2015	NUM
ecletica-56	275	23	.	.	PUNCT
ecletica-56	276	1	69	69	NUM
ecletica-56	276	2	69	69	NUM
ecletica-56	277	1	[	[	X
ecletica-56	277	2	19	19	NUM
ecletica-56	277	3	]	]	X
ecletica-56	277	4	n.c	n.c	PROPN
ecletica-56	277	5	.	.	PROPN
ecletica-56	277	6	merbel	merbel	PROPN
ecletica-56	277	7	,	,	PUNCT
ecletica-56	277	8	g.	g.	PROPN
ecletica-56	277	9	wilkens	wilkens	PROPN
ecletica-56	277	10	,	,	PUNCT
ecletica-56	277	11	s.	s.	PROPN
ecletica-56	277	12	fowles	fowles	PROPN
ecletica-56	277	13	,	,	PUNCT
ecletica-56	277	14	b.	b.	PROPN
ecletica-56	277	15	oosterhuis	oosterhuis	PROPN
ecletica-56	277	16	,	,	PUNCT
ecletica-56	277	17	j.h.g	j.h.g	PROPN
ecletica-56	277	18	.	.	PUNCT
ecletica-56	277	19	jonkman	jonkman	PROPN
ecletica-56	277	20	,	,	PUNCT
ecletica-56	277	21	lc	lc	NOUN
ecletica-56	277	22	phases	phase	NOUN
ecletica-56	277	23	improve	improve	VERB
ecletica-56	277	24	,	,	PUNCT
ecletica-56	277	25	but	but	CCONJ
ecletica-56	277	26	not	not	PART
ecletica-56	277	27	all	all	DET
ecletica-56	277	28	assays	assay	NOUN
ecletica-56	277	29	do	do	VERB
ecletica-56	277	30	:	:	PUNCT
ecletica-56	277	31	metformin	metformin	NOUN
ecletica-56	277	32	bioanalysis	bioanalysis	NOUN
ecletica-56	277	33	revisited	revisit	VERB
ecletica-56	277	34	,	,	PUNCT
ecletica-56	277	35	chromatographia	chromatographia	NOUN
ecletica-56	277	36	,	,	PUNCT
ecletica-56	277	37	47(1998	47(1998	NUM
ecletica-56	277	38	)	)	PUNCT
ecletica-56	277	39	542	542	NUM
ecletica-56	277	40	-	-	SYM
ecletica-56	277	41	546	546	NUM
ecletica-56	277	42	.	.	PUNCT
ecletica-56	278	1	[	[	X
ecletica-56	278	2	20	20	NUM
ecletica-56	278	3	]	]	X
ecletica-56	278	4	m.s	m.s	PROPN
ecletica-56	278	5	.	.	PROPN
ecletica-56	278	6	arayne	arayne	PROPN
ecletica-56	278	7	,	,	PUNCT
ecletica-56	278	8	n.	n.	PROPN
ecletica-56	278	9	sulbana	sulbana	PROPN
ecletica-56	278	10	,	,	PUNCT
ecletica-56	278	11	m.h	m.h	PROPN
ecletica-56	278	12	.	.	PROPN
ecletica-56	278	13	zuberi	zuberi	PROPN
ecletica-56	278	14	,	,	PUNCT
ecletica-56	278	15	development	development	NOUN
ecletica-56	278	16	and	and	CCONJ
ecletica-56	278	17	validation	validation	NOUN
ecletica-56	278	18	of	of	ADP
ecletica-56	278	19	rp	rp	NOUN
ecletica-56	278	20	-	-	PUNCT
ecletica-56	278	21	hplc	hplc	NOUN
ecletica-56	278	22	method	method	NOUN
ecletica-56	278	23	for	for	ADP
ecletica-56	278	24	the	the	DET
ecletica-56	278	25	analysis	analysis	NOUN
ecletica-56	278	26	of	of	ADP
ecletica-56	278	27	metformin	metformin	NOUN
ecletica-56	278	28	,	,	PUNCT
ecletica-56	278	29	pak	pak	PROPN
ecletica-56	278	30	.	.	PUNCT
ecletica-56	279	1	j.	j.	PROPN
ecletica-56	279	2	pharm	pharm	PROPN
ecletica-56	279	3	.	.	PUNCT
ecletica-56	280	1	sci	sci	PROPN
ecletica-56	280	2	.	.	PROPN
ecletica-56	281	1	19	19	NUM
ecletica-56	281	2	(	(	PUNCT
ecletica-56	281	3	2006	2006	NUM
ecletica-56	281	4	)	)	PUNCT
ecletica-56	281	5	231	231	NUM
ecletica-56	281	6	-	-	SYM
ecletica-56	281	7	234	234	NUM
ecletica-56	281	8	.	.	PUNCT
ecletica-56	282	1	[	[	X
ecletica-56	282	2	21	21	NUM
ecletica-56	282	3	]	]	X
ecletica-56	282	4	j.j	j.j	PROPN
ecletica-56	282	5	.	.	PROPN
ecletica-56	282	6	jiang	jiang	PROPN
ecletica-56	282	7	,	,	PUNCT
ecletica-56	282	8	f.	f.	PROPN
ecletica-56	282	9	feng	feng	PROPN
ecletica-56	282	10	,	,	PUNCT
ecletica-56	282	11	m.	m.	PROPN
ecletica-56	282	12	ma	ma	PROPN
ecletica-56	282	13	,	,	PUNCT
ecletica-56	282	14	z.x	z.x	PROPN
ecletica-56	282	15	.	.	PROPN
ecletica-56	282	16	zhang	zhang	PROPN
ecletica-56	282	17	,	,	PUNCT
ecletica-56	282	18	study	study	VERB
ecletica-56	282	19	on	on	ADP
ecletica-56	282	20	a	a	DET
ecletica-56	282	21	new	new	ADJ
ecletica-56	282	22	precolumn	precolumn	NOUN
ecletica-56	282	23	derivatization	derivatization	NOUN
ecletica-56	282	24	method	method	NOUN
ecletica-56	282	25	in	in	ADP
ecletica-56	282	26	the	the	DET
ecletica-56	282	27	determination	determination	NOUN
ecletica-56	282	28	of	of	ADP
ecletica-56	282	29	metformin	metformin	NOUN
ecletica-56	282	30	hydrochloride	hydrochloride	NOUN
ecletica-56	282	31	,	,	PUNCT
ecletica-56	282	32	j.	j.	PROPN
ecletica-56	282	33	chromatogr	chromatogr	PROPN
ecletica-56	282	34	.	.	PUNCT
ecletica-56	283	1	sci	sci	PROPN
ecletica-56	283	2	.	.	PROPN
ecletica-56	284	1	44	44	NUM
ecletica-56	284	2	(	(	PUNCT
ecletica-56	284	3	2006	2006	NUM
ecletica-56	284	4	)	)	PUNCT
ecletica-56	284	5	193	193	NUM
ecletica-56	284	6	-	-	SYM
ecletica-56	284	7	199	199	NUM
ecletica-56	284	8	.	.	PUNCT
ecletica-56	285	1	[	[	X
ecletica-56	285	2	22	22	NUM
ecletica-56	285	3	]	]	SYM
ecletica-56	285	4	f.tache	f.tache	NOUN
ecletica-56	285	5	,	,	PUNCT
ecletica-56	285	6	m.	m.	NOUN
ecletica-56	285	7	albu	albu	PROPN
ecletica-56	285	8	,	,	PUNCT
ecletica-56	285	9	specificity	specificity	NOUN
ecletica-56	285	10	of	of	ADP
ecletica-56	285	11	an	an	DET
ecletica-56	285	12	analytical	analytical	ADJ
ecletica-56	285	13	hplc	hplc	NOUN
ecletica-56	285	14	assay	assay	NOUN
ecletica-56	285	15	method	method	NOUN
ecletica-56	285	16	of	of	ADP
ecletica-56	285	17	metformin	metformin	NOUN
ecletica-56	285	18	hydrochloride	hydrochloride	NOUN
ecletica-56	285	19	,	,	PUNCT
ecletica-56	285	20	rev	rev	PROPN
ecletica-56	285	21	.	.	PROPN
ecletica-56	285	22	roum	roum	PROPN
ecletica-56	285	23	.	.	PUNCT
ecletica-56	286	1	chim	chim	PROPN
ecletica-56	286	2	.	.	PUNCT
ecletica-56	287	1	52(2007	52(2007	NUM
ecletica-56	287	2	)	)	PUNCT
ecletica-56	287	3	603	603	NUM
ecletica-56	287	4	-	-	SYM
ecletica-56	287	5	609	609	NUM
ecletica-56	287	6	.	.	PUNCT
ecletica-56	288	1	[	[	X
ecletica-56	288	2	23	23	NUM
ecletica-56	288	3	]	]	X
ecletica-56	288	4	s.	s.	PROPN
ecletica-56	288	5	tanabe	tanabe	PROPN
ecletica-56	288	6	,	,	PUNCT
ecletica-56	288	7	t.	t.	PROPN
ecletica-56	288	8	kobayashi	kobayashi	PROPN
ecletica-56	288	9	,	,	PUNCT
ecletica-56	288	10	k.	k.	PROPN
ecletica-56	288	11	kawanabe	kawanabe	PROPN
ecletica-56	288	12	,	,	PUNCT
ecletica-56	288	13	determination	determination	NOUN
ecletica-56	288	14	of	of	ADP
ecletica-56	288	15	oral	oral	ADJ
ecletica-56	288	16	hypoglycemic	hypoglycemic	ADJ
ecletica-56	288	17	biguanides	biguanide	NOUN
ecletica-56	288	18	by	by	ADP
ecletica-56	288	19	high	high	ADJ
ecletica-56	288	20	performance	performance	NOUN
ecletica-56	288	21	liquid	liquid	NOUN
ecletica-56	288	22	chromatography	chromatography	NOUN
ecletica-56	288	23	with	with	ADP
ecletica-56	288	24	fluorescence	fluorescence	NOUN
ecletica-56	288	25	detection	detection	NOUN
ecletica-56	288	26	,	,	PUNCT
ecletica-56	288	27	anal	anal	NOUN
ecletica-56	288	28	.	.	PUNCT
ecletica-56	289	1	sci	sci	PROPN
ecletica-56	289	2	.	.	PUNCT
ecletica-56	290	1	3(1987	3(1987	NUM
ecletica-56	290	2	)	)	PUNCT
ecletica-56	290	3	69	69	NUM
ecletica-56	290	4	-	-	SYM
ecletica-56	290	5	73	73	NUM
ecletica-56	290	6	.	.	PUNCT
ecletica-56	291	1	[	[	X
ecletica-56	291	2	24	24	NUM
ecletica-56	291	3	]	]	PUNCT
ecletica-56	291	4	m.vasudevan	m.vasudevan	NOUN
ecletica-56	291	5	,	,	PUNCT
ecletica-56	291	6	j.	j.	PROPN
ecletica-56	291	7	ravi	ravi	PROPN
ecletica-56	291	8	,	,	PUNCT
ecletica-56	291	9	s.	s.	PROPN
ecletica-56	291	10	ravisankar	ravisankar	PROPN
ecletica-56	291	11	,	,	PUNCT
ecletica-56	291	12	b.	b.	PROPN
ecletica-56	291	13	surreh	surreh	PROPN
ecletica-56	291	14	,	,	PUNCT
ecletica-56	291	15	ion	ion	NOUN
ecletica-56	291	16	-	-	PUNCT
ecletica-56	291	17	par	par	NOUN
ecletica-56	291	18	liquid	liquid	ADJ
ecletica-56	291	19	chromatography	chromatography	NOUN
ecletica-56	291	20	technique	technique	NOUN
ecletica-56	291	21	for	for	ADP
ecletica-56	291	22	the	the	DET
ecletica-56	291	23	estimation	estimation	NOUN
ecletica-56	291	24	of	of	ADP
ecletica-56	291	25	metformin	metformin	NOUN
ecletica-56	291	26	in	in	ADP
ecletica-56	291	27	its	its	PRON
ecletica-56	291	28	multicomponent	multicomponent	NOUN
ecletica-56	291	29	dosage	dosage	NOUN
ecletica-56	291	30	forms	form	NOUN
ecletica-56	291	31	,	,	PUNCT
ecletica-56	291	32	j.	j.	PROPN
ecletica-56	291	33	pharmac	pharmac	PROPN
ecletica-56	291	34	.	.	PUNCT
ecletica-56	292	1	biochem	biochem	PROPN
ecletica-56	292	2	.	.	PUNCT
ecletica-56	293	1	anal	anal	ADJ
ecletica-56	293	2	.	.	PUNCT
ecletica-56	294	1	25	25	NUM
ecletica-56	294	2	(	(	PUNCT
ecletica-56	294	3	2001	2001	NUM
ecletica-56	294	4	)	)	PUNCT
ecletica-56	294	5	77	77	NUM
ecletica-56	294	6	-	-	SYM
ecletica-56	294	7	84	84	NUM
ecletica-56	294	8	.	.	PUNCT
ecletica-56	295	1	[	[	X
ecletica-56	295	2	25	25	NUM
ecletica-56	295	3	]	]	X
ecletica-56	295	4	n.r	n.r	PROPN
ecletica-56	295	5	.	.	PROPN
ecletica-56	295	6	lad	lad	PROPN
ecletica-56	295	7	,	,	PUNCT
ecletica-56	295	8	s.i	s.i	PROPN
ecletica-56	295	9	.	.	PROPN
ecletica-56	295	10	bhoir	bhoir	PROPN
ecletica-56	295	11	,	,	PUNCT
ecletica-56	295	12	i.c	i.c	PROPN
ecletica-56	295	13	.	.	PROPN
ecletica-56	295	14	bhoir	bhoir	PROPN
ecletica-56	295	15	,	,	PUNCT
ecletica-56	295	16	m.	m.	NOUN
ecletica-56	295	17	sundaresan	sundaresan	PROPN
ecletica-56	295	18	,	,	PUNCT
ecletica-56	295	19	concurrent	concurrent	ADJ
ecletica-56	295	20	assay	assay	NOUN
ecletica-56	295	21	of	of	ADP
ecletica-56	295	22	metformin	metformin	NOUN
ecletica-56	295	23	and	and	CCONJ
ecletica-56	295	24	glimepiride	glimepiride	NOUN
ecletica-56	295	25	in	in	ADP
ecletica-56	295	26	tablets	tablet	NOUN
ecletica-56	295	27	using	use	VERB
ecletica-56	295	28	rp	rp	NOUN
ecletica-56	295	29	-	-	PUNCT
ecletica-56	295	30	hplc	hplc	NOUN
ecletica-56	295	31	with	with	ADP
ecletica-56	295	32	wave	wave	NOUN
ecletica-56	295	33	length	length	NOUN
ecletica-56	295	34	programming	programming	NOUN
ecletica-56	295	35	,	,	PUNCT
ecletica-56	295	36	indian	indian	PROPN
ecletica-56	295	37	j.	j.	PROPN
ecletica-56	295	38	pharma	pharma	PROPN
ecletica-56	295	39	.	.	PUNCT
ecletica-56	296	1	sci	sci	PROPN
ecletica-56	296	2	.	.	PROPN
ecletica-56	297	1	65	65	NUM
ecletica-56	297	2	(	(	PUNCT
ecletica-56	297	3	2003	2003	NUM
ecletica-56	297	4	)	)	PUNCT
ecletica-56	297	5	650	650	NUM
ecletica-56	297	6	-	-	PUNCT
ecletica-56	297	7	653	653	NUM
ecletica-56	297	8	.	.	PUNCT
ecletica-56	298	1	[	[	X
ecletica-56	298	2	26	26	NUM
ecletica-56	298	3	]	]	X
ecletica-56	298	4	b.	b.	PROPN
ecletica-56	298	5	l.	l.	PROPN
ecletica-56	298	6	kolte	kolte	PROPN
ecletica-56	298	7	,	,	PUNCT
ecletica-56	298	8	b.b	b.b	PROPN
ecletica-56	298	9	.	.	PROPN
ecletica-56	298	10	raut	raut	PROPN
ecletica-56	298	11	,	,	PUNCT
ecletica-56	298	12	a.a	a.a	PROPN
ecletica-56	298	13	.	.	PROPN
ecletica-56	298	14	deo	deo	PROPN
ecletica-56	298	15	,	,	PUNCT
ecletica-56	298	16	m.a	m.a	PROPN
ecletica-56	298	17	.	.	PROPN
ecletica-56	298	18	bagool	bagool	PROPN
ecletica-56	298	19	,	,	PUNCT
ecletica-56	298	20	m.	m.	NOUN
ecletica-56	298	21	a.	a.	PROPN
ecletica-56	298	22	,	,	PUNCT
ecletica-56	298	23	d.b	d.b	PROPN
ecletica-56	298	24	.	.	PROPN
ecletica-56	298	25	shinde	shinde	PROPN
ecletica-56	298	26	,	,	PUNCT
ecletica-56	298	27	simultaneous	simultaneous	ADJ
ecletica-56	298	28	determination	determination	NOUN
ecletica-56	298	29	of	of	ADP
ecletica-56	298	30	metformin	metformin	NOUN
ecletica-56	298	31	in	in	ADP
ecletica-56	298	32	its	its	PRON
ecletica-56	298	33	multicomponent	multicomponent	NOUN
ecletica-56	298	34	dosage	dosage	NOUN
ecletica-56	298	35	forms	form	NOUN
ecletica-56	298	36	with	with	ADP
ecletica-56	298	37	glizipide	glizipide	NOUN
ecletica-56	298	38	and	and	CCONJ
ecletica-56	298	39	gliclazide	gliclazide	NOUN
ecletica-56	298	40	using	use	VERB
ecletica-56	298	41	micellar	micellar	ADJ
ecletica-56	298	42	liquid	liquid	ADJ
ecletica-56	298	43	chromatography	chromatography	NOUN
ecletica-56	298	44	,	,	PUNCT
ecletica-56	298	45	j.	j.	PROPN
ecletica-56	298	46	liquid	liquid	ADJ
ecletica-56	298	47	chromatogr	chromatogr	PROPN
ecletica-56	298	48	.	.	PUNCT
ecletica-56	299	1	related	related	ADJ
ecletica-56	299	2	techonol	techonol	NOUN
ecletica-56	299	3	.	.	PUNCT
ecletica-56	300	1	26	26	NUM
ecletica-56	300	2	(	(	PUNCT
ecletica-56	300	3	2003	2003	NUM
ecletica-56	300	4	)	)	PUNCT
ecletica-56	300	5	1117	1117	NUM
ecletica-56	300	6	-	-	SYM
ecletica-56	300	7	1133	1133	NUM
ecletica-56	300	8	.	.	PUNCT
ecletica-56	301	1	[	[	X
ecletica-56	301	2	27	27	NUM
ecletica-56	301	3	]	]	X
ecletica-56	301	4	b.l	b.l	PROPN
ecletica-56	301	5	.	.	PROPN
ecletica-56	301	6	kolte	kolte	PROPN
ecletica-56	301	7	,	,	PUNCT
ecletica-56	301	8	b.b	b.b	PROPN
ecletica-56	301	9	.	.	PROPN
ecletica-56	301	10	raut	raut	PROPN
ecletica-56	301	11	,	,	PUNCT
ecletica-56	301	12	a.a	a.a	PROPN
ecletica-56	301	13	.	.	PROPN
ecletica-56	301	14	deo	deo	PROPN
ecletica-56	301	15	,	,	PUNCT
ecletica-56	301	16	m.a	m.a	PROPN
ecletica-56	301	17	.	.	PROPN
ecletica-56	301	18	bagool	bagool	PROPN
ecletica-56	301	19	,	,	PUNCT
ecletica-56	301	20	d.b	d.b	PROPN
ecletica-56	301	21	.	.	PROPN
ecletica-56	301	22	shinde	shinde	PROPN
ecletica-56	301	23	,	,	PUNCT
ecletica-56	301	24	simultaneous	simultaneous	ADJ
ecletica-56	301	25	determination	determination	NOUN
ecletica-56	301	26	of	of	ADP
ecletica-56	301	27	metformin	metformin	NOUN
ecletica-56	301	28	in	in	ADP
ecletica-56	301	29	combination	combination	NOUN
ecletica-56	301	30	with	with	ADP
ecletica-56	301	31	rosiglitazone	rosiglitazone	NOUN
ecletica-56	301	32	by	by	ADP
ecletica-56	301	33	reversed	reverse	VERB
ecletica-56	301	34	-	-	PUNCT
ecletica-56	301	35	phase	phase	NOUN
ecletica-56	301	36	liquid	liquid	ADJ
ecletica-56	301	37	chromatography	chromatography	NOUN
ecletica-56	301	38	,	,	PUNCT
ecletica-56	301	39	j.	j.	PROPN
ecletica-56	301	40	chromatogr	chromatogr	PROPN
ecletica-56	301	41	.	.	PUNCT
ecletica-56	302	1	sci	sci	PROPN
ecletica-56	302	2	.	.	PUNCT
ecletica-56	302	3	42(2004	42(2004	PROPN
ecletica-56	302	4	)	)	PUNCT
ecletica-56	302	5	70	70	NUM
ecletica-56	302	6	-	-	SYM
ecletica-56	302	7	73	73	NUM
ecletica-56	302	8	.	.	PUNCT
ecletica-56	303	1	[	[	X
ecletica-56	303	2	28	28	NUM
ecletica-56	303	3	]	]	X
ecletica-56	303	4	a.	a.	NOUN
ecletica-56	303	5	dubey	dubey	PROPN
ecletica-56	303	6	,	,	PUNCT
ecletica-56	303	7	i.c	i.c	PROPN
ecletica-56	303	8	.	.	PROPN
ecletica-56	303	9	shukla	shukla	PROPN
ecletica-56	303	10	,	,	PUNCT
ecletica-56	303	11	simultaneous	simultaneous	ADJ
ecletica-56	303	12	determination	determination	NOUN
ecletica-56	303	13	of	of	ADP
ecletica-56	303	14	glipizide	glipizide	NOUN
ecletica-56	303	15	and	and	CCONJ
ecletica-56	303	16	metformin	metformin	NOUN
ecletica-56	303	17	hydrochloride	hydrochloride	NOUN
ecletica-56	303	18	in	in	ADP
ecletica-56	303	19	pharmaceutical	pharmaceutical	ADJ
ecletica-56	303	20	preparation	preparation	NOUN
ecletica-56	303	21	by	by	ADP
ecletica-56	303	22	hplc	hplc	PROPN
ecletica-56	303	23	,	,	PUNCT
ecletica-56	303	24	j.	j.	PROPN
ecletica-56	303	25	indian	indian	PROPN
ecletica-56	303	26	chem	chem	PROPN
ecletica-56	303	27	.	.	PUNCT
ecletica-56	304	1	soc	soc	PROPN
ecletica-56	304	2	.	.	PUNCT
ecletica-56	305	1	81(2004	81(2004	NUM
ecletica-56	305	2	)	)	PUNCT
ecletica-56	305	3	,	,	PUNCT
ecletica-56	305	4	84	84	NUM
ecletica-56	305	5	-	-	SYM
ecletica-56	305	6	86	86	NUM
ecletica-56	305	7	.	.	PUNCT
ecletica-56	306	1	[	[	X
ecletica-56	306	2	29	29	NUM
ecletica-56	306	3	]	]	X
ecletica-56	306	4	b.l	b.l	PROPN
ecletica-56	306	5	.	.	PROPN
ecletica-56	306	6	kolte	kolte	PROPN
ecletica-56	306	7	,	,	PUNCT
ecletica-56	306	8	b.b	b.b	PROPN
ecletica-56	306	9	.	.	PROPN
ecletica-56	306	10	raut	raut	PROPN
ecletica-56	306	11	,	,	PUNCT
ecletica-56	306	12	a.a	a.a	PROPN
ecletica-56	306	13	.	.	PROPN
ecletica-56	306	14	deo	deo	PROPN
ecletica-56	306	15	,	,	PUNCT
ecletica-56	306	16	m.a	m.a	PROPN
ecletica-56	306	17	.	.	PROPN
ecletica-56	306	18	bagool	bagool	PROPN
ecletica-56	306	19	,	,	PUNCT
ecletica-56	306	20	d.b	d.b	PROPN
ecletica-56	306	21	.	.	PROPN
ecletica-56	306	22	shinde	shinde	PROPN
ecletica-56	306	23	,	,	PUNCT
ecletica-56	306	24	simultaneous	simultaneous	ADJ
ecletica-56	306	25	determination	determination	NOUN
ecletica-56	306	26	of	of	ADP
ecletica-56	306	27	metformin	metformin	NOUN
ecletica-56	306	28	and	and	CCONJ
ecletica-56	306	29	glimepride	glimepride	NOUN
ecletica-56	306	30	in	in	ADP
ecletica-56	306	31	pharmaceutical	pharmaceutical	ADJ
ecletica-56	306	32	dosage	dosage	NOUN
ecletica-56	306	33	form	form	NOUN
ecletica-56	306	34	by	by	ADP
ecletica-56	306	35	reverse	reverse	NOUN
ecletica-56	306	36	-	-	PUNCT
ecletica-56	306	37	phase	phase	NOUN
ecletica-56	306	38	liquid	liquid	ADJ
ecletica-56	306	39	chromatography	chromatography	NOUN
ecletica-56	306	40	,	,	PUNCT
ecletica-56	306	41	j.	j.	PROPN
ecletica-56	306	42	separation	separation	PROPN
ecletica-56	306	43	sci	sci	PROPN
ecletica-56	306	44	.	.	PROPN
ecletica-56	306	45	28	28	NUM
ecletica-56	306	46	(	(	PUNCT
ecletica-56	306	47	2005	2005	NUM
ecletica-56	306	48	)	)	PUNCT
ecletica-56	306	49	2076	2076	NUM
ecletica-56	306	50	-	-	SYM
ecletica-56	306	51	2079	2079	NUM
ecletica-56	306	52	.	.	PUNCT
ecletica-56	307	1	[	[	X
ecletica-56	307	2	30	30	NUM
ecletica-56	307	3	]	]	X
ecletica-56	307	4	m.b	m.b	PROPN
ecletica-56	307	5	.	.	PROPN
ecletica-56	307	6	shankar	shankar	PROPN
ecletica-56	307	7	,	,	PUNCT
ecletica-56	307	8	v.d	v.d	PROPN
ecletica-56	307	9	.	.	PROPN
ecletica-56	307	10	modi	modi	PROPN
ecletica-56	307	11	,	,	PUNCT
ecletica-56	307	12	d.a	d.a	PROPN
ecletica-56	307	13	.	.	PROPN
ecletica-56	307	14	shaah	shaah	PROPN
ecletica-56	307	15	,	,	PUNCT
ecletica-56	307	16	k.k	k.k	PROPN
ecletica-56	307	17	.	.	PROPN
ecletica-56	307	18	bhatt	bhatt	PROPN
ecletica-56	307	19	,	,	PUNCT
ecletica-56	307	20	r.s	r.s	PROPN
ecletica-56	307	21	.	.	PROPN
ecletica-56	307	22	mehta	mehta	PROPN
ecletica-56	307	23	,	,	PUNCT
ecletica-56	307	24	m.	m.	NOUN
ecletica-56	307	25	geetha	geetha	PROPN
ecletica-56	307	26	,	,	PUNCT
ecletica-56	307	27	b.j	b.j	PROPN
ecletica-56	307	28	.	.	PROPN
ecletica-56	307	29	patel	patel	PROPN
ecletica-56	307	30	,	,	PUNCT
ecletica-56	307	31	estimation	estimation	NOUN
ecletica-56	307	32	of	of	ADP
ecletica-56	307	33	pioglitazone	pioglitazone	NOUN
ecletica-56	307	34	hydrocloride	hydrocloride	ADV
ecletica-56	307	35	and	and	CCONJ
ecletica-56	307	36	metformin	metformin	NOUN
ecletica-56	307	37	hydrocloride	hydrocloride	ADV
ecletica-56	307	38	in	in	ADP
ecletica-56	307	39	tablets	tablet	NOUN
ecletica-56	307	40	by	by	ADP
ecletica-56	307	41	derivative	derivative	ADJ
ecletica-56	307	42	spectrophometry	spectrophometry	NOUN
ecletica-56	307	43	and	and	CCONJ
ecletica-56	307	44	liquid	liquid	ADJ
ecletica-56	307	45	chromatographic	chromatographic	ADJ
ecletica-56	307	46	methods	method	NOUN
ecletica-56	307	47	,	,	PUNCT
ecletica-56	307	48	j.aoac	j.aoac	VERB
ecletica-56	307	49	int	int	NOUN
ecletica-56	307	50	.	.	PUNCT
ecletica-56	308	1	88	88	NUM
ecletica-56	308	2	(	(	PUNCT
ecletica-56	308	3	2005	2005	NUM
ecletica-56	308	4	)	)	PUNCT
ecletica-56	308	5	1167	1167	NUM
ecletica-56	308	6	-	-	SYM
ecletica-56	308	7	1172	1172	NUM
ecletica-56	308	8	.	.	PUNCT
ecletica-56	309	1	[	[	X
ecletica-56	309	2	31	31	NUM
ecletica-56	309	3	]	]	X
ecletica-56	309	4	b.	b.	PROPN
ecletica-56	309	5	m.	m.	PROPN
ecletica-56	309	6	rahman	rahman	PROPN
ecletica-56	309	7	,	,	PUNCT
ecletica-56	309	8	m.m	m.m	PROPN
ecletica-56	309	9	.	.	PROPN
ecletica-56	309	10	rahman	rahman	PROPN
ecletica-56	309	11	,	,	PUNCT
ecletica-56	309	12	m.ahmed	m.ahmed	PROPN
ecletica-56	309	13	,	,	PUNCT
ecletica-56	309	14	m.r	m.r	PROPN
ecletica-56	309	15	.	.	PROPN
ecletica-56	309	16	islam	islam	PROPN
ecletica-56	309	17	,	,	PUNCT
ecletica-56	309	18	wahed	wahed	PROPN
ecletica-56	309	19	,	,	PUNCT
ecletica-56	309	20	m.i.i	m.i.i	NOUN
ecletica-56	309	21	.	.	PROPN
ecletica-56	309	22	,	,	PUNCT
ecletica-56	309	23	r.k	r.k	PROPN
ecletica-56	309	24	.	.	PROPN
ecletica-56	309	25	barman	barman	PROPN
ecletica-56	309	26	,	,	PUNCT
ecletica-56	309	27	m.a.r	m.a.r	NOUN
ecletica-56	309	28	.	.	PUNCT
ecletica-56	310	1	khan	khan	PROPN
ecletica-56	310	2	,	,	PUNCT
ecletica-56	310	3	m.b	m.b	PROPN
ecletica-56	310	4	.	.	PROPN
ecletica-56	310	5	hossain	hossain	PROPN
ecletica-56	310	6	,	,	PUNCT
ecletica-56	310	7	m.s	m.s	PROPN
ecletica-56	310	8	.	.	PROPN
ecletica-56	310	9	amran	amran	PROPN
ecletica-56	310	10	,	,	PUNCT
ecletica-56	310	11	simultaneous	simultaneous	ADJ
ecletica-56	310	12	high	high	ADJ
ecletica-56	310	13	-	-	PUNCT
ecletica-56	310	14	performance	performance	NOUN
ecletica-56	310	15	liquid	liquid	ADJ
ecletica-56	310	16	chromatographic	chromatographic	ADJ
ecletica-56	310	17	determination	determination	NOUN
ecletica-56	310	18	of	of	ADP
ecletica-56	310	19	metformin	metformin	NOUN
ecletica-56	310	20	hydrochloride	hydrochloride	NOUN
ecletica-56	310	21	and	and	CCONJ
ecletica-56	310	22	rosiglitazone	rosiglitazone	NOUN
ecletica-56	310	23	maleate	maleate	NOUN
ecletica-56	310	24	in	in	ADP
ecletica-56	310	25	pharmaceutical	pharmaceutical	NOUN
ecletica-56	310	26	-	-	PUNCT
ecletica-56	310	27	dosage	dosage	NOUN
ecletica-56	310	28	form	form	NOUN
ecletica-56	310	29	,	,	PUNCT
ecletica-56	310	30	res	re	NOUN
ecletica-56	310	31	.	.	PUNCT
ecletica-56	311	1	j.	j.	PROPN
ecletica-56	311	2	med	med	PROPN
ecletica-56	311	3	.	.	PUNCT
ecletica-56	312	1	med	med	PROPN
ecletica-56	312	2	.	.	PUNCT
ecletica-56	313	1	sci	sci	PROPN
ecletica-56	313	2	.	.	PROPN
ecletica-56	313	3	2	2	NUM
ecletica-56	313	4	(	(	PUNCT
ecletica-56	313	5	2007	2007	NUM
ecletica-56	313	6	)	)	PUNCT
ecletica-56	313	7	115	115	NUM
ecletica-56	313	8	-	-	SYM
ecletica-56	313	9	121	121	NUM
ecletica-56	313	10	.	.	PUNCT
ecletica-56	314	1	[	[	X
ecletica-56	314	2	32	32	NUM
ecletica-56	314	3	]	]	PUNCT
ecletica-56	314	4	d.	d.	PROPN
ecletica-56	314	5	jain	jain	PROPN
ecletica-56	314	6	,	,	PUNCT
ecletica-56	314	7	s.	s.	PROPN
ecletica-56	314	8	jain	jain	PROPN
ecletica-56	314	9	,	,	PUNCT
ecletica-56	314	10	m.	m.	NOUN
ecletica-56	314	11	amin	amin	PROPN
ecletica-56	314	12	,	,	PUNCT
ecletica-56	314	13	simultaneous	simultaneous	ADJ
ecletica-56	314	14	estimation	estimation	NOUN
ecletica-56	314	15	of	of	ADP
ecletica-56	314	16	metformin	metformin	NOUN
ecletica-56	314	17	hydrochloride	hydrochloride	NOUN
ecletica-56	314	18	,	,	PUNCT
ecletica-56	314	19	pioglitazone	pioglitazone	NOUN
ecletica-56	314	20	hydrochloride	hydrochloride	NOUN
ecletica-56	314	21	,	,	PUNCT
ecletica-56	314	22	and	and	CCONJ
ecletica-56	314	23	glimepiride	glimepiride	NOUN
ecletica-56	314	24	by	by	ADP
ecletica-56	314	25	rp	rp	NOUN
ecletica-56	314	26	-	-	PUNCT
ecletica-56	314	27	hplc	hplc	NOUN
ecletica-56	314	28	in	in	ADP
ecletica-56	314	29	tablet	tablet	ADJ
ecletica-56	314	30	formulation	formulation	NOUN
ecletica-56	314	31	,	,	PUNCT
ecletica-56	314	32	j.	j.	PROPN
ecletica-56	314	33	chromatogr	chromatogr	PROPN
ecletica-56	314	34	.	.	PUNCT
ecletica-56	315	1	sci	sci	PROPN
ecletica-56	315	2	.	.	PUNCT
ecletica-56	315	3	46(2008	46(2008	PROPN
ecletica-56	315	4	)	)	PUNCT
ecletica-56	315	5	501	501	NUM
ecletica-56	315	6	-	-	SYM
ecletica-56	315	7	506	506	NUM
ecletica-56	315	8	.	.	PUNCT
ecletica-56	316	1	[	[	X
ecletica-56	316	2	33	33	NUM
ecletica-56	316	3	]	]	X
ecletica-56	316	4	p.k	p.k	PROPN
ecletica-56	316	5	.	.	PROPN
ecletica-56	316	6	sahoo	sahoo	PROPN
ecletica-56	316	7	,	,	PUNCT
ecletica-56	316	8	r.	r.	PROPN
ecletica-56	316	9	sharma	sharma	PROPN
ecletica-56	316	10	,	,	PUNCT
ecletica-56	316	11	s.c	s.c	PROPN
ecletica-56	316	12	.	.	PROPN
ecletica-56	316	13	chaturvedi	chaturvedi	PROPN
ecletica-56	316	14	,	,	PUNCT
ecletica-56	316	15	simultaneous	simultaneous	ADJ
ecletica-56	316	16	estimation	estimation	NOUN
ecletica-56	316	17	of	of	ADP
ecletica-56	316	18	metformin	metformin	NOUN
ecletica-56	316	19	hydrochloride	hydrochloride	NOUN
ecletica-56	316	20	and	and	CCONJ
ecletica-56	316	21	pioglitazone	pioglitazone	NOUN
ecletica-56	316	22	hydrochloride	hydrochloride	NOUN
ecletica-56	316	23	by	by	ADP
ecletica-56	316	24	rphplc	rphplc	NOUN
ecletica-56	316	25	method	method	NOUN
ecletica-56	316	26	from	from	ADP
ecletica-56	316	27	combined	combine	VERB
ecletica-56	316	28	tablet	tablet	NOUN
ecletica-56	316	29	dosage	dosage	NOUN
ecletica-56	316	30	form	form	NOUN
ecletica-56	316	31	,	,	PUNCT
ecletica-56	316	32	indian	indian	PROPN
ecletica-56	316	33	.	.	PUNCT
ecletica-56	317	1	j.	j.	PROPN
ecletica-56	317	2	pharm	pharm	PROPN
ecletica-56	317	3	.	.	PUNCT
ecletica-56	318	1	sci	sci	PROPN
ecletica-56	318	2	.	.	PROPN
ecletica-56	319	1	70	70	NUM
ecletica-56	319	2	(	(	PUNCT
ecletica-56	319	3	2008	2008	NUM
ecletica-56	319	4	)	)	PUNCT
ecletica-56	319	5	383	383	NUM
ecletica-56	319	6	-	-	SYM
ecletica-56	319	7	386	386	NUM
ecletica-56	319	8	.	.	PUNCT
ecletica-56	320	1	eclética	eclética	PROPN
ecletica-56	320	2	química	química	PROPN
ecletica-56	320	3	,	,	PUNCT
ecletica-56	320	4	vol	vol	NOUN
ecletica-56	320	5	.	.	PROPN
ecletica-56	320	6	40	40	NUM
ecletica-56	320	7	,	,	PUNCT
ecletica-56	320	8	62	62	NUM
ecletica-56	320	9	-	-	SYM
ecletica-56	320	10	70	70	NUM
ecletica-56	320	11	,	,	PUNCT
ecletica-56	320	12	2015	2015	NUM
ecletica-56	320	13	.	.	PUNCT
ecletica-56	321	1	70	70	NUM
ecletica-56	321	2	70	70	NUM
ecletica-56	321	3	[	[	X
ecletica-56	321	4	34	34	NUM
ecletica-56	321	5	]	]	PUNCT
ecletica-56	321	6	m.	m.	NOUN
ecletica-56	321	7	tubino	tubino	NOUN
ecletica-56	321	8	,	,	PUNCT
ecletica-56	321	9	l.f	l.f	PROPN
ecletica-56	321	10	.	.	PROPN
ecletica-56	321	11	bianchessi	bianchessi	PROPN
ecletica-56	321	12	,	,	PUNCT
ecletica-56	321	13	m.m.d.c	m.m.d.c	PROPN
ecletica-56	321	14	.	.	PROPN
ecletica-56	321	15	vila	vila	PROPN
ecletica-56	321	16	,	,	PUNCT
ecletica-56	321	17	quantitative	quantitative	ADJ
ecletica-56	321	18	spot	spot	NOUN
ecletica-56	321	19	-	-	PUNCT
ecletica-56	321	20	test	test	NOUN
ecletica-56	321	21	analysis	analysis	NOUN
ecletica-56	321	22	of	of	ADP
ecletica-56	321	23	metformin	metformin	NOUN
ecletica-56	321	24	in	in	ADP
ecletica-56	321	25	pharmaceutical	pharmaceutical	ADJ
ecletica-56	321	26	preparations	preparation	NOUN
ecletica-56	321	27	,	,	PUNCT
ecletica-56	321	28	anal	anal	NOUN
ecletica-56	321	29	.	.	PUNCT
ecletica-56	322	1	sci	sci	PROPN
ecletica-56	322	2	.	.	PROPN
ecletica-56	323	1	26	26	NUM
ecletica-56	323	2	(	(	PUNCT
ecletica-56	323	3	2010	2010	NUM
ecletica-56	323	4	)	)	PUNCT
ecletica-56	323	5	121	121	NUM
ecletica-56	323	6	-	-	SYM
ecletica-56	323	7	124	124	NUM
ecletica-56	323	8	.	.	PUNCT
ecletica-56	324	1	[	[	X
ecletica-56	324	2	35	35	NUM
ecletica-56	324	3	]	]	PUNCT
ecletica-56	324	4	m.	m.	NOUN
ecletica-56	324	5	tubino	tubino	NOUN
ecletica-56	324	6	,	,	PUNCT
ecletica-56	324	7	r.l	r.l	PROPN
ecletica-56	324	8	.	.	PROPN
ecletica-56	324	9	souza	souza	PROPN
ecletica-56	324	10	,	,	PUNCT
ecletica-56	324	11	gravimetric	gravimetric	ADJ
ecletica-56	324	12	method	method	NOUN
ecletica-56	324	13	for	for	ADP
ecletica-56	324	14	the	the	DET
ecletica-56	324	15	determination	determination	NOUN
ecletica-56	324	16	of	of	ADP
ecletica-56	324	17	diclofenac	diclofenac	NOUN
ecletica-56	324	18	in	in	ADP
ecletica-56	324	19	pharmaceutical	pharmaceutical	ADJ
ecletica-56	324	20	preparations	preparation	NOUN
ecletica-56	324	21	.	.	PUNCT
ecletica-56	325	1	j.	j.	PROPN
ecletica-56	325	2	aoac	aoac	PROPN
ecletica-56	325	3	int	int	PROPN
ecletica-56	325	4	.	.	PUNCT
ecletica-56	326	1	88	88	NUM
ecletica-56	326	2	(	(	PUNCT
ecletica-56	326	3	2005	2005	NUM
ecletica-56	326	4	)	)	PUNCT
ecletica-56	326	5	1684	1684	NUM
ecletica-56	326	6	-	-	SYM
ecletica-56	326	7	1687	1687	NUM
ecletica-56	326	8	.	.	PUNCT
ecletica-56	327	1	[	[	X
ecletica-56	327	2	36	36	NUM
ecletica-56	327	3	]	]	PUNCT
ecletica-56	327	4	k.	k.	NOUN
ecletica-56	327	5	eckschlager	eckschlager	PROPN
ecletica-56	327	6	,	,	PUNCT
ecletica-56	327	7	errors	error	NOUN
ecletica-56	327	8	,	,	PUNCT
ecletica-56	327	9	measurement	measurement	NOUN
ecletica-56	327	10	and	and	CCONJ
ecletica-56	327	11	results	result	NOUN
ecletica-56	327	12	in	in	ADP
ecletica-56	327	13	chemical	chemical	ADJ
ecletica-56	327	14	analysis	analysis	NOUN
ecletica-56	327	15	,	,	PUNCT
ecletica-56	327	16	van	van	PROPN
ecletica-56	327	17	nostrand	nostrand	PROPN
ecletica-56	327	18	reinhold	reinhold	PROPN
ecletica-56	327	19	company	company	PROPN
ecletica-56	327	20	,	,	PUNCT
ecletica-56	327	21	london	london	PROPN
ecletica-56	327	22	,	,	PUNCT
ecletica-56	327	23	1972	1972	NUM
ecletica-56	327	24	,	,	PUNCT
ecletica-56	327	25	pp	pp	ADJ
ecletica-56	327	26	.	.	PUNCT
ecletica-56	327	27	109	109	NUM
ecletica-56	327	28	-	-	SYM
ecletica-56	327	29	120	120	NUM
ecletica-56	327	30	.	.	PUNCT