id	sid	tid	token	lemma	pos
ecletica-640	1	1	eclética	eclética	PROPN
ecletica-640	1	2	química	química	PROPN
ecletica-640	1	3	print	print	PROPN
ecletica-640	1	4	version	version	PROPN
ecletica-640	1	5	issn	issn	PROPN
ecletica-640	1	6	0100	0100	NUM
ecletica-640	1	7	-	-	PUNCT
ecletica-640	1	8	4670on	4670on	NOUN
ecletica-640	1	9	-	-	PUNCT
ecletica-640	1	10	line	line	NOUN
ecletica-640	1	11	version	version	NOUN
ecletica-640	1	12	issn	issn	PROPN
ecletica-640	1	13	1678	1678	NUM
ecletica-640	1	14	-	-	SYM
ecletica-640	1	15	4618	4618	NUM
ecletica-640	1	16	eclet	eclet	NOUN
ecletica-640	1	17	.	.	PUNCT
ecletica-640	2	1	quím	quím	NOUN
ecletica-640	2	2	.	.	PUNCT
ecletica-640	3	1	vol.26	vol.26	ADJ
ecletica-640	3	2	são	são	PROPN
ecletica-640	3	3	paulo	paulo	PROPN
ecletica-640	3	4	2001	2001	NUM
ecletica-640	3	5	http://dx.doi.org/10.1590/s0100-46702001000100005	http://dx.doi.org/10.1590/s0100-46702001000100005	PROPN
ecletica-640	3	6	model	model	PROPN
ecletica-640	3	7	studies	study	NOUN
ecletica-640	3	8	on	on	ADP
ecletica-640	3	9	the	the	DET
ecletica-640	3	10	synthesis	synthesis	NOUN
ecletica-640	3	11	of	of	ADP
ecletica-640	3	12	the	the	DET
ecletica-640	3	13	natural	natural	ADJ
ecletica-640	3	14	meroterpenoid	meroterpenoid	NOUN
ecletica-640	3	15	cordiaquinone	cordiaquinone	PROPN
ecletica-640	3	16	a	a	DET
ecletica-640	3	17	claudemir	claudemir	NOUN
ecletica-640	3	18	batalini	batalini	PROPN
ecletica-640	3	19	*	*	PUNCT
ecletica-640	3	20	lothar	lothar	PROPN
ecletica-640	3	21	wilhelm	wilhelm	PROPN
ecletica-640	3	22	bieber	bieber	PROPN
ecletica-640	4	1	*	*	PROPN
ecletica-640	4	2	*	*	PUNCT
ecletica-640	5	1	abstract	abstract	NOUN
ecletica-640	5	2	:	:	PUNCT
ecletica-640	5	3	two	two	NUM
ecletica-640	5	4	main	main	ADJ
ecletica-640	5	5	strategies	strategy	NOUN
ecletica-640	5	6	for	for	ADP
ecletica-640	5	7	the	the	DET
ecletica-640	5	8	synthesis	synthesis	NOUN
ecletica-640	5	9	of	of	ADP
ecletica-640	5	10	the	the	DET
ecletica-640	5	11	natural	natural	ADJ
ecletica-640	5	12	meroterpenoid	meroterpenoid	NOUN
ecletica-640	5	13	cordiaquinone	cordiaquinone	NOUN
ecletica-640	5	14	a	a	PRON
ecletica-640	5	15	(	(	PUNCT
ecletica-640	5	16	1	1	NUM
ecletica-640	5	17	)	)	PUNCT
ecletica-640	5	18	isolated	isolate	VERB
ecletica-640	5	19	of	of	ADP
ecletica-640	5	20	the	the	DET
ecletica-640	5	21	roots	root	NOUN
ecletica-640	5	22	of	of	ADP
ecletica-640	5	23	cordia	cordia	PROPN
ecletica-640	5	24	corymbosa	corymbosa	PROPN
ecletica-640	5	25	g.	g.	PROPN
ecletica-640	5	26	don	don	PROPN
ecletica-640	5	27	(	(	PUNCT
ecletica-640	5	28	boraginaceae	boraginaceae	PROPN
ecletica-640	5	29	)	)	PUNCT
ecletica-640	5	30	were	be	AUX
ecletica-640	5	31	tested	test	VERB
ecletica-640	5	32	on	on	ADP
ecletica-640	5	33	model	model	NOUN
ecletica-640	5	34	compounds	compound	NOUN
ecletica-640	5	35	.	.	PUNCT
ecletica-640	6	1	whereas	whereas	SCONJ
ecletica-640	6	2	all	all	DET
ecletica-640	6	3	attempts	attempt	NOUN
ecletica-640	6	4	of	of	ADP
ecletica-640	6	5	alkylation	alkylation	NOUN
ecletica-640	6	6	of	of	ADP
ecletica-640	6	7	e	e	NOUN
ecletica-640	6	8	-	-	NOUN
ecletica-640	6	9	caprolactone	caprolactone	ADJ
ecletica-640	6	10	(	(	PUNCT
ecletica-640	6	11	10	10	NUM
ecletica-640	6	12	)	)	PUNCT
ecletica-640	6	13	were	be	AUX
ecletica-640	6	14	unsuccessful	unsuccessful	ADJ
ecletica-640	6	15	,	,	PUNCT
ecletica-640	6	16	the	the	DET
ecletica-640	6	17	coupling	coupling	NOUN
ecletica-640	6	18	of	of	ADP
ecletica-640	6	19	epoxycitronellol	epoxycitronellol	NOUN
ecletica-640	6	20	(	(	PUNCT
ecletica-640	6	21	17	17	NUM
ecletica-640	6	22	)	)	PUNCT
ecletica-640	6	23	with	with	ADP
ecletica-640	6	24	an	an	DET
ecletica-640	6	25	appropriate	appropriate	ADJ
ecletica-640	6	26	organocuprate	organocuprate	NOUN
ecletica-640	6	27	proceeded	proceed	VERB
ecletica-640	6	28	in	in	ADP
ecletica-640	6	29	the	the	DET
ecletica-640	6	30	expected	expect	VERB
ecletica-640	6	31	direction	direction	NOUN
ecletica-640	6	32	.	.	PUNCT
ecletica-640	7	1	keywords	keyword	NOUN
ecletica-640	7	2	:	:	PUNCT
ecletica-640	7	3	meroterpenoid	meroterpenoid	NOUN
ecletica-640	7	4	naphthoquinone	naphthoquinone	NOUN
ecletica-640	7	5	,	,	PUNCT
ecletica-640	7	6	cordia	cordia	PROPN
ecletica-640	7	7	corymbosa	corymbosa	PROPN
ecletica-640	7	8	,	,	PUNCT
ecletica-640	7	9	boraginaceae	boraginaceae	NOUN
ecletica-640	7	10	,	,	PUNCT
ecletica-640	7	11	e	e	NOUN
ecletica-640	7	12	-	-	NOUN
ecletica-640	7	13	caprolactone	caprolactone	ADJ
ecletica-640	7	14	,	,	PUNCT
ecletica-640	7	15	epoxycitronellol	epoxycitronellol	NOUN
ecletica-640	7	16	,	,	PUNCT
ecletica-640	7	17	organocuprate	organocuprate	NOUN
ecletica-640	7	18	.	.	PUNCT
ecletica-640	8	1	introduction	introduction	NOUN
ecletica-640	8	2	cordiaquinone	cordiaquinone	PROPN
ecletica-640	8	3	a	a	PRON
ecletica-640	8	4	(	(	PUNCT
ecletica-640	8	5	1	1	NUM
ecletica-640	8	6	)	)	PUNCT
ecletica-640	8	7	is	be	AUX
ecletica-640	8	8	the	the	DET
ecletica-640	8	9	most	most	ADV
ecletica-640	8	10	abundant	abundant	ADJ
ecletica-640	8	11	of	of	ADP
ecletica-640	8	12	a	a	DET
ecletica-640	8	13	new	new	ADJ
ecletica-640	8	14	type	type	NOUN
ecletica-640	8	15	of	of	ADP
ecletica-640	8	16	meroterpenoid	meroterpenoid	NOUN
ecletica-640	8	17	naphthoquinones	naphthoquinone	NOUN
ecletica-640	8	18	found	find	VERB
ecletica-640	8	19	in	in	ADP
ecletica-640	8	20	the	the	DET
ecletica-640	8	21	roots	root	NOUN
ecletica-640	8	22	of	of	ADP
ecletica-640	8	23	cordia	cordia	PROPN
ecletica-640	8	24	corymbosa	corymbosa	PROPN
ecletica-640	8	25	g.	g.	PROPN
ecletica-640	8	26	don	don	PROPN
ecletica-640	8	27	,	,	PUNCT
ecletica-640	8	28	popularly	popularly	ADV
ecletica-640	8	29	known	know	VERB
ecletica-640	8	30	as	as	ADP
ecletica-640	8	31	"	"	PUNCT
ecletica-640	8	32	maria	maria	NOUN
ecletica-640	8	33	preta".2,3	preta".2,3	NOUN
ecletica-640	8	34	the	the	DET
ecletica-640	8	35	unique	unique	ADJ
ecletica-640	8	36	rearranged	rearrange	VERB
ecletica-640	8	37	terpenoid	terpenoid	NOUN
ecletica-640	8	38	skeleton	skeleton	NOUN
ecletica-640	8	39	of	of	ADP
ecletica-640	8	40	still	still	ADV
ecletica-640	8	41	unknown	unknown	ADJ
ecletica-640	8	42	absolute	absolute	ADJ
ecletica-640	8	43	configuration	configuration	NOUN
ecletica-640	8	44	represents	represent	VERB
ecletica-640	8	45	an	an	DET
ecletica-640	8	46	interesting	interesting	ADJ
ecletica-640	8	47	challenge	challenge	NOUN
ecletica-640	8	48	for	for	ADP
ecletica-640	8	49	an	an	DET
ecletica-640	8	50	asymmetric	asymmetric	ADJ
ecletica-640	8	51	total	total	ADJ
ecletica-640	8	52	synthesis	synthesis	NOUN
ecletica-640	8	53	which	which	PRON
ecletica-640	8	54	should	should	AUX
ecletica-640	8	55	start	start	VERB
ecletica-640	8	56	with	with	ADP
ecletica-640	8	57	a	a	DET
ecletica-640	8	58	simple	simple	ADJ
ecletica-640	8	59	,	,	PUNCT
ecletica-640	8	60	enantiomerically	enantiomerically	ADV
ecletica-640	8	61	pure	pure	ADJ
ecletica-640	8	62	and	and	CCONJ
ecletica-640	8	63	easily	easily	ADV
ecletica-640	8	64	available	available	ADJ
ecletica-640	8	65	compound	compound	NOUN
ecletica-640	8	66	.	.	PUNCT
ecletica-640	9	1	a	a	DET
ecletica-640	9	2	first	first	ADJ
ecletica-640	9	3	retrosynthetic	retrosynthetic	ADJ
ecletica-640	9	4	analysis	analysis	NOUN
ecletica-640	9	5	(	(	PUNCT
ecletica-640	9	6	scheme	scheme	NOUN
ecletica-640	9	7	1	1	NUM
ecletica-640	9	8	)	)	PUNCT
ecletica-640	9	9	suggested	suggest	VERB
ecletica-640	9	10	the	the	DET
ecletica-640	9	11	unfunctionalizated	unfunctionalizated	ADJ
ecletica-640	9	12	naphthalene	naphthalene	NOUN
ecletica-640	9	13	(	(	PUNCT
ecletica-640	9	14	2	2	NUM
ecletica-640	9	15	)	)	PUNCT
ecletica-640	9	16	as	as	ADP
ecletica-640	9	17	the	the	DET
ecletica-640	9	18	most	most	ADV
ecletica-640	9	19	suitable	suitable	ADJ
ecletica-640	9	20	precursor	precursor	NOUN
ecletica-640	9	21	because	because	SCONJ
ecletica-640	9	22	of	of	ADP
ecletica-640	9	23	the	the	DET
ecletica-640	9	24	availability	availability	NOUN
ecletica-640	9	25	of	of	ADP
ecletica-640	9	26	a	a	DET
ecletica-640	9	27	number	number	NOUN
ecletica-640	9	28	of	of	ADP
ecletica-640	9	29	simple	simple	ADJ
ecletica-640	9	30	2	2	NUM
ecletica-640	9	31	-	-	PUNCT
ecletica-640	9	32	substituted	substitute	VERB
ecletica-640	9	33	naphthalenes	naphthalene	NOUN
ecletica-640	9	34	which	which	PRON
ecletica-640	9	35	could	could	AUX
ecletica-640	9	36	be	be	AUX
ecletica-640	9	37	used	use	VERB
ecletica-640	9	38	as	as	ADP
ecletica-640	9	39	building	build	VERB
ecletica-640	9	40	blocks	block	NOUN
ecletica-640	9	41	.	.	PUNCT
ecletica-640	10	1	however	however	ADV
ecletica-640	10	2	,	,	PUNCT
ecletica-640	10	3	the	the	DET
ecletica-640	10	4	final	final	ADJ
ecletica-640	10	5	oxydation	oxydation	NOUN
ecletica-640	10	6	(	(	PUNCT
ecletica-640	10	7	probably	probably	ADV
ecletica-640	10	8	by	by	ADP
ecletica-640	10	9	ce4	ce4	PROPN
ecletica-640	10	10	+	+	PROPN
ecletica-640	10	11	)	)	PUNCT
ecletica-640	10	12	is	be	AUX
ecletica-640	10	13	not	not	PART
ecletica-640	10	14	expected	expect	VERB
ecletica-640	10	15	to	to	PART
ecletica-640	10	16	be	be	AUX
ecletica-640	10	17	regioselective.12	regioselective.12	NOUN
ecletica-640	10	18	for	for	ADP
ecletica-640	10	19	the	the	DET
ecletica-640	10	20	next	next	ADJ
ecletica-640	10	21	step	step	NOUN
ecletica-640	10	22	,	,	PUNCT
ecletica-640	10	23	the	the	DET
ecletica-640	10	24	introduction	introduction	NOUN
ecletica-640	10	25	of	of	ADP
ecletica-640	10	26	a	a	DET
ecletica-640	10	27	tetrasubstituted	tetrasubstitute	VERB
ecletica-640	10	28	olefinic	olefinic	ADJ
ecletica-640	10	29	double	double	ADJ
ecletica-640	10	30	bond	bond	NOUN
ecletica-640	10	31	,	,	PUNCT
ecletica-640	10	32	a	a	DET
ecletica-640	10	33	wittig	wittig	NOUN
ecletica-640	10	34	-	-	PUNCT
ecletica-640	10	35	reaction	reaction	NOUN
ecletica-640	10	36	was	be	AUX
ecletica-640	10	37	not	not	PART
ecletica-640	10	38	considered	consider	VERB
ecletica-640	10	39	because	because	SCONJ
ecletica-640	10	40	of	of	ADP
ecletica-640	10	41	the	the	DET
ecletica-640	10	42	risk	risk	NOUN
ecletica-640	10	43	of	of	ADP
ecletica-640	10	44	epimerization	epimerization	NOUN
ecletica-640	10	45	a	a	PRON
ecletica-640	10	46	to	to	ADP
ecletica-640	10	47	the	the	DET
ecletica-640	10	48	carbonyl	carbonyl	NOUN
ecletica-640	10	49	group	group	NOUN
ecletica-640	10	50	in	in	ADP
ecletica-640	10	51	the	the	DET
ecletica-640	10	52	case	case	NOUN
ecletica-640	10	53	of	of	ADP
ecletica-640	10	54	the	the	DET
ecletica-640	10	55	use	use	NOUN
ecletica-640	10	56	of	of	ADP
ecletica-640	10	57	pure	pure	ADJ
ecletica-640	10	58	enantiomers	enantiomer	NOUN
ecletica-640	10	59	.	.	PUNCT
ecletica-640	11	1	water	water	NOUN
ecletica-640	11	2	elimination	elimination	NOUN
ecletica-640	11	3	from	from	ADP
ecletica-640	11	4	the	the	DET
ecletica-640	11	5	tertiary	tertiary	ADJ
ecletica-640	11	6	alcohol	alcohol	NOUN
ecletica-640	11	7	(	(	PUNCT
ecletica-640	11	8	3	3	NUM
ecletica-640	11	9	)	)	PUNCT
ecletica-640	11	10	seemed	seem	VERB
ecletica-640	11	11	more	more	ADV
ecletica-640	11	12	reliable	reliable	ADJ
ecletica-640	11	13	.	.	PUNCT
ecletica-640	12	1	this	this	DET
ecletica-640	12	2	diol	diol	NOUN
ecletica-640	12	3	offers	offer	VERB
ecletica-640	12	4	two	two	NUM
ecletica-640	12	5	very	very	ADV
ecletica-640	12	6	short	short	ADJ
ecletica-640	12	7	alternatives	alternative	NOUN
ecletica-640	12	8	of	of	ADP
ecletica-640	12	9	disconnection	disconnection	NOUN
ecletica-640	12	10	to	to	ADP
ecletica-640	12	11	simple	simple	ADJ
ecletica-640	12	12	starting	start	VERB
ecletica-640	12	13	materials	material	NOUN
ecletica-640	12	14	:	:	PUNCT
ecletica-640	13	1	1	1	X
ecletica-640	13	2	.	.	PUNCT
ecletica-640	13	3	the	the	DET
ecletica-640	13	4	addition	addition	NOUN
ecletica-640	13	5	of	of	ADP
ecletica-640	13	6	methyl	methyl	NOUN
ecletica-640	13	7	lithium	lithium	NOUN
ecletica-640	13	8	to	to	ADP
ecletica-640	13	9	a	a	DET
ecletica-640	13	10	carboxylic	carboxylic	ADJ
ecletica-640	13	11	intermediate	intermediate	ADJ
ecletica-640	13	12	,	,	PUNCT
ecletica-640	13	13	ideally	ideally	ADV
ecletica-640	13	14	the	the	DET
ecletica-640	13	15	substituted	substitute	VERB
ecletica-640	13	16	http://www.scielo.br/scielo.php?script=sci_serial&pid=0100-4670&lng=en&nrm=iso	http://www.scielo.br/scielo.php?script=sci_serial&pid=0100-4670&lng=en&nrm=iso	NOUN
ecletica-640	13	17	http://www.scielo.br/scielo.php?script=sci_arttext&pid=s0100-46702001000100005&lng=en&nrm=iso&tlng=en#nota02	http://www.scielo.br/scielo.php?script=sci_arttext&pid=s0100-46702001000100005&lng=en&nrm=iso&tlng=en#nota02	NUM
ecletica-640	13	18	http://www.scielo.br/scielo.php?script=sci_arttext&pid=s0100-46702001000100005&lng=en&nrm=iso&tlng=en#nota01	http://www.scielo.br/scielo.php?script=sci_arttext&pid=s0100-46702001000100005&lng=en&nrm=iso&tlng=en#nota01	NOUN
ecletica-640	13	19	lactone	lactone	NOUN
ecletica-640	13	20	(	(	PUNCT
ecletica-640	13	21	4	4	NUM
ecletica-640	13	22	)	)	PUNCT
ecletica-640	13	23	which	which	PRON
ecletica-640	13	24	should	should	AUX
ecletica-640	13	25	be	be	AUX
ecletica-640	13	26	accessible	accessible	ADJ
ecletica-640	13	27	from	from	ADP
ecletica-640	13	28	3	3	NUM
ecletica-640	13	29	-	-	PUNCT
ecletica-640	13	30	methyl	methyl	NOUN
ecletica-640	13	31	-	-	PUNCT
ecletica-640	13	32	e	e	NOUN
ecletica-640	13	33	-	-	NOUN
ecletica-640	13	34	caprolactone	caprolactone	ADJ
ecletica-640	13	35	(	(	PUNCT
ecletica-640	13	36	5	5	NUM
ecletica-640	13	37	)	)	PUNCT
ecletica-640	13	38	and	and	CCONJ
ecletica-640	13	39	a	a	DET
ecletica-640	13	40	suitable	suitable	ADJ
ecletica-640	13	41	alkylating	alkylate	VERB
ecletica-640	13	42	agent	agent	NOUN
ecletica-640	13	43	(	(	PUNCT
ecletica-640	13	44	6).1,7	6).1,7	NUM
ecletica-640	13	45	both	both	CCONJ
ecletica-640	13	46	pure	pure	ADJ
ecletica-640	13	47	enantiomers	enantiomer	NOUN
ecletica-640	13	48	of	of	ADP
ecletica-640	13	49	(	(	PUNCT
ecletica-640	13	50	5	5	NUM
ecletica-640	13	51	)	)	PUNCT
ecletica-640	13	52	have	have	AUX
ecletica-640	13	53	been	be	AUX
ecletica-640	13	54	prepared	prepare	VERB
ecletica-640	13	55	before	before	ADV
ecletica-640	13	56	from	from	ADP
ecletica-640	13	57	pulegone.8	pulegone.8	PROPN
ecletica-640	13	58	2	2	NUM
ecletica-640	13	59	.	.	PUNCT
ecletica-640	14	1	the	the	DET
ecletica-640	14	2	nucleophilic	nucleophilic	ADJ
ecletica-640	14	3	ring	ring	NOUN
ecletica-640	14	4	opening	opening	NOUN
ecletica-640	14	5	10	10	NUM
ecletica-640	14	6	of	of	ADP
ecletica-640	14	7	the	the	DET
ecletica-640	14	8	epoxide	epoxide	NOUN
ecletica-640	14	9	(	(	PUNCT
ecletica-640	14	10	7	7	NUM
ecletica-640	14	11	)	)	PUNCT
ecletica-640	14	12	with	with	ADP
ecletica-640	14	13	a	a	DET
ecletica-640	14	14	conjugate	conjugate	ADJ
ecletica-640	14	15	cuprate	cuprate	NOUN
ecletica-640	14	16	(	(	PUNCT
ecletica-640	14	17	8)	8)	NUM
ecletica-640	14	18	derived	derive	VERB
ecletica-640	14	19	from	from	ADP
ecletica-640	14	20	(	(	PUNCT
ecletica-640	14	21	6	6	NUM
ecletica-640	14	22	)	)	PUNCT
ecletica-640	14	23	.	.	PUNCT
ecletica-640	15	1	(	(	PUNCT
ecletica-640	15	2	7	7	X
ecletica-640	15	3	)	)	PUNCT
ecletica-640	15	4	may	may	AUX
ecletica-640	15	5	be	be	AUX
ecletica-640	15	6	obtained	obtain	VERB
ecletica-640	15	7	from	from	ADP
ecletica-640	15	8	the	the	DET
ecletica-640	15	9	known	know	VERB
ecletica-640	15	10	unsaturated	unsaturated	ADJ
ecletica-640	15	11	alcohol	alcohol	NOUN
ecletica-640	15	12	(	(	PUNCT
ecletica-640	15	13	9	9	NUM
ecletica-640	15	14	)	)	PUNCT
ecletica-640	15	15	,	,	PUNCT
ecletica-640	15	16	previously	previously	ADV
ecletica-640	15	17	described	describe	VERB
ecletica-640	15	18	as	as	ADP
ecletica-640	15	19	a	a	DET
ecletica-640	15	20	subproduct	subproduct	NOUN
ecletica-640	15	21	of	of	ADP
ecletica-640	15	22	a	a	DET
ecletica-640	15	23	multistep	multistep	ADJ
ecletica-640	15	24	procedure	procedure	NOUN
ecletica-640	15	25	starting	start	VERB
ecletica-640	15	26	from	from	ADP
ecletica-640	15	27	b	b	NOUN
ecletica-640	15	28	-	-	PUNCT
ecletica-640	15	29	pinene.13	pinene.13	NOUN
ecletica-640	15	30	material	material	NOUN
ecletica-640	15	31	and	and	CCONJ
ecletica-640	15	32	method	method	NOUN
ecletica-640	15	33	melting	melting	NOUN
ecletica-640	15	34	points	point	NOUN
ecletica-640	15	35	are	be	AUX
ecletica-640	15	36	uncorrected	uncorrecte	VERB
ecletica-640	15	37	.	.	PUNCT
ecletica-640	16	1	nmr1h	nmr1h	PROPN
ecletica-640	16	2	spectra	spectra	PROPN
ecletica-640	16	3	were	be	AUX
ecletica-640	16	4	recorded	record	VERB
ecletica-640	16	5	on	on	ADP
ecletica-640	16	6	a	a	DET
ecletica-640	16	7	varian	varian	NOUN
ecletica-640	16	8	em	em	PRON
ecletica-640	16	9	390	390	NUM
ecletica-640	16	10	instrument	instrument	NOUN
ecletica-640	16	11	at	at	ADP
ecletica-640	16	12	90	90	NUM
ecletica-640	16	13	mhz	mhz	NOUN
ecletica-640	16	14	.	.	PUNCT
ecletica-640	17	1	ir	ir	PROPN
ecletica-640	17	2	spectra	spectra	PROPN
ecletica-640	17	3	were	be	AUX
ecletica-640	17	4	obtained	obtain	VERB
ecletica-640	17	5	on	on	ADP
ecletica-640	17	6	a	a	DET
ecletica-640	17	7	bruker	bruker	PROPN
ecletica-640	17	8	ftir	ftir	PROPN
ecletica-640	17	9	ifs	ifs	PROPN
ecletica-640	17	10	66	66	NUM
ecletica-640	17	11	spectrometer	spectrometer	NOUN
ecletica-640	17	12	.	.	PUNCT
ecletica-640	18	1	thf	thf	NOUN
ecletica-640	18	2	was	be	AUX
ecletica-640	18	3	distilled	distil	VERB
ecletica-640	18	4	over	over	ADP
ecletica-640	18	5	metallic	metallic	ADJ
ecletica-640	18	6	potassium	potassium	NOUN
ecletica-640	18	7	before	before	ADP
ecletica-640	18	8	use	use	NOUN
ecletica-640	18	9	.	.	PUNCT
ecletica-640	19	1	all	all	DET
ecletica-640	19	2	new	new	ADJ
ecletica-640	19	3	compounds	compound	NOUN
ecletica-640	19	4	–	–	PUNCT
ecletica-640	19	5	(	(	PUNCT
ecletica-640	19	6	6	6	NUM
ecletica-640	19	7	)	)	PUNCT
ecletica-640	19	8	(	(	PUNCT
ecletica-640	19	9	x	x	X
ecletica-640	19	10	=	=	VERB
ecletica-640	19	11	i	i	PROPN
ecletica-640	19	12	)	)	PUNCT
ecletica-640	19	13	,	,	PUNCT
ecletica-640	19	14	(	(	PUNCT
ecletica-640	19	15	12	12	NUM
ecletica-640	19	16	)	)	PUNCT
ecletica-640	19	17	,	,	PUNCT
ecletica-640	19	18	(	(	PUNCT
ecletica-640	19	19	13	13	NUM
ecletica-640	19	20	)	)	PUNCT
ecletica-640	19	21	,	,	PUNCT
ecletica-640	19	22	(	(	PUNCT
ecletica-640	19	23	15	15	NUM
ecletica-640	19	24	)	)	PUNCT
ecletica-640	19	25	and	and	CCONJ
ecletica-640	19	26	(	(	PUNCT
ecletica-640	19	27	18	18	NUM
ecletica-640	19	28	)	)	PUNCT
ecletica-640	19	29	–	–	PUNCT
ecletica-640	19	30	gave	give	VERB
ecletica-640	19	31	satisfactory	satisfactory	ADJ
ecletica-640	19	32	elemental	elemental	ADJ
ecletica-640	19	33	analyses	analysis	NOUN
ecletica-640	19	34	.	.	PUNCT
ecletica-640	20	1	2-(2	2-(2	NOUN
ecletica-640	20	2	-	-	PUNCT
ecletica-640	20	3	iodoethyl	iodoethyl	PROPN
ecletica-640	20	4	)	)	PUNCT
ecletica-640	20	5	naphthalene	naphthalene	NOUN
ecletica-640	20	6	(	(	PUNCT
ecletica-640	20	7	6	6	NUM
ecletica-640	20	8	,	,	PUNCT
ecletica-640	20	9	x	x	PUNCT
ecletica-640	20	10	=	=	VERB
ecletica-640	21	1	i	i	PROPN
ecletica-640	21	2	):	):	PUNCT
ecletica-640	21	3	3.0	3.0	NUM
ecletica-640	21	4	mmol	mmol	NOUN
ecletica-640	21	5	(	(	PUNCT
ecletica-640	21	6	0.45	0.45	NUM
ecletica-640	21	7	g	g	NOUN
ecletica-640	21	8	)	)	PUNCT
ecletica-640	21	9	of	of	ADP
ecletica-640	21	10	sodium	sodium	NOUN
ecletica-640	21	11	iodide	iodide	NOUN
ecletica-640	21	12	and	and	CCONJ
ecletica-640	21	13	3.0	3.0	NUM
ecletica-640	21	14	mmol	mmol	NOUN
ecletica-640	21	15	(	(	PUNCT
ecletica-640	21	16	0.97	0.97	NUM
ecletica-640	21	17	g	g	NOUN
ecletica-640	21	18	)	)	PUNCT
ecletica-640	21	19	of	of	ADP
ecletica-640	21	20	toluenesulfonate	toluenesulfonate	NOUN
ecletica-640	21	21	(	(	PUNCT
ecletica-640	21	22	6	6	NUM
ecletica-640	21	23	)	)	PUNCT
ecletica-640	21	24	(	(	PUNCT
ecletica-640	21	25	x	x	X
ecletica-640	21	26	=	=	SYM
ecletica-640	21	27	otos	oto	VERB
ecletica-640	21	28	)	)	PUNCT
ecletica-640	21	29	1	1	NUM
ecletica-640	21	30	were	be	AUX
ecletica-640	21	31	stirred	stir	VERB
ecletica-640	21	32	in	in	ADP
ecletica-640	21	33	10	10	NUM
ecletica-640	21	34	ml	ml	NOUN
ecletica-640	21	35	of	of	ADP
ecletica-640	21	36	acetone	acetone	NOUN
ecletica-640	21	37	in	in	ADP
ecletica-640	21	38	the	the	DET
ecletica-640	21	39	dark	dark	NOUN
ecletica-640	21	40	.	.	PUNCT
ecletica-640	22	1	after	after	ADP
ecletica-640	22	2	3	3	NUM
ecletica-640	22	3	days	day	NOUN
ecletica-640	22	4	,	,	PUNCT
ecletica-640	22	5	30	30	NUM
ecletica-640	22	6	ml	ml	NOUN
ecletica-640	22	7	of	of	ADP
ecletica-640	22	8	hexane	hexane	NOUN
ecletica-640	22	9	were	be	AUX
ecletica-640	22	10	added	add	VERB
ecletica-640	22	11	and	and	CCONJ
ecletica-640	22	12	the	the	DET
ecletica-640	22	13	mixture	mixture	NOUN
ecletica-640	22	14	was	be	AUX
ecletica-640	22	15	allowed	allow	VERB
ecletica-640	22	16	to	to	PART
ecletica-640	22	17	stand	stand	VERB
ecletica-640	22	18	for	for	ADP
ecletica-640	22	19	2	2	NUM
ecletica-640	22	20	h.	h.	NOUN
ecletica-640	22	21	the	the	DET
ecletica-640	22	22	precipitate	precipitate	NOUN
ecletica-640	22	23	was	be	AUX
ecletica-640	22	24	filtered	filter	VERB
ecletica-640	22	25	off	off	ADP
ecletica-640	22	26	and	and	CCONJ
ecletica-640	22	27	the	the	DET
ecletica-640	22	28	solvent	solvent	NOUN
ecletica-640	22	29	was	be	AUX
ecletica-640	22	30	evaporated	evaporate	VERB
ecletica-640	22	31	.	.	PUNCT
ecletica-640	23	1	the	the	DET
ecletica-640	23	2	residue	residue	NOUN
ecletica-640	23	3	was	be	AUX
ecletica-640	23	4	recrystallized	recrystallize	VERB
ecletica-640	23	5	from	from	ADP
ecletica-640	23	6	15	15	NUM
ecletica-640	23	7	ml	ml	NOUN
ecletica-640	23	8	of	of	ADP
ecletica-640	23	9	hexane	hexane	NOUN
ecletica-640	23	10	.	.	PUNCT
ecletica-640	24	1	yield	yield	NOUN
ecletica-640	24	2	:	:	PUNCT
ecletica-640	24	3	0.65	0.65	NUM
ecletica-640	24	4	g	g	NOUN
ecletica-640	24	5	(	(	PUNCT
ecletica-640	24	6	77	77	NUM
ecletica-640	24	7	%	%	NOUN
ecletica-640	24	8	)	)	PUNCT
ecletica-640	24	9	of	of	ADP
ecletica-640	24	10	colourless	colourless	ADJ
ecletica-640	24	11	needles	needle	NOUN
ecletica-640	24	12	,	,	PUNCT
ecletica-640	24	13	m.p	m.p	PROPN
ecletica-640	24	14	.	.	PROPN
ecletica-640	24	15	82	82	NUM
ecletica-640	24	16	-	-	SYM
ecletica-640	24	17	83	83	NUM
ecletica-640	24	18	°	°	PROPN
ecletica-640	24	19	c.	c.	PROPN
ecletica-640	24	20	nmr1h	nmr1h	PROPN
ecletica-640	24	21	(	(	PUNCT
ecletica-640	24	22	ccl4	ccl4	PROPN
ecletica-640	24	23	)	)	PUNCT
ecletica-640	25	1	d	d	NOUN
ecletica-640	25	2	:	:	PUNCT
ecletica-640	25	3	3.45	3.45	NUM
ecletica-640	25	4	(	(	PUNCT
ecletica-640	25	5	s	s	PROPN
ecletica-640	25	6	,	,	PUNCT
ecletica-640	25	7	4h	4h	NOUN
ecletica-640	25	8	)	)	PUNCT
ecletica-640	25	9	;	;	PUNCT
ecletica-640	25	10	7.30	7.30	NUM
ecletica-640	25	11	-	-	SYM
ecletica-640	25	12	8.10	8.10	NUM
ecletica-640	25	13	(	(	PUNCT
ecletica-640	25	14	m	m	PROPN
ecletica-640	25	15	,	,	PUNCT
ecletica-640	25	16	7h	7h	NUM
ecletica-640	25	17	)	)	PUNCT
ecletica-640	25	18	.	.	PUNCT
ecletica-640	26	1	3	3	X
ecletica-640	26	2	-	-	PUNCT
ecletica-640	26	3	methoxycarbonyl-2	methoxycarbonyl-2	NOUN
ecletica-640	26	4	-	-	PUNCT
ecletica-640	26	5	oxepanone	oxepanone	NOUN
ecletica-640	26	6	(	(	PUNCT
ecletica-640	26	7	12	12	NUM
ecletica-640	26	8	):	):	PUNCT
ecletica-640	26	9	to	to	ADP
ecletica-640	26	10	a	a	DET
ecletica-640	26	11	solution	solution	NOUN
ecletica-640	26	12	of	of	ADP
ecletica-640	26	13	20.0	20.0	NUM
ecletica-640	26	14	mmol	mmol	NOUN
ecletica-640	26	15	(	(	PUNCT
ecletica-640	26	16	2.8	2.8	NUM
ecletica-640	26	17	ml	ml	NOUN
ecletica-640	26	18	)	)	PUNCT
ecletica-640	26	19	of	of	ADP
ecletica-640	26	20	dry	dry	ADJ
ecletica-640	26	21	diisopropylamine	diisopropylamine	NOUN
ecletica-640	26	22	in	in	ADP
ecletica-640	26	23	20	20	NUM
ecletica-640	26	24	ml	ml	NOUN
ecletica-640	26	25	of	of	ADP
ecletica-640	26	26	thf	thf	NOUN
ecletica-640	26	27	,	,	PUNCT
ecletica-640	26	28	at	at	ADP
ecletica-640	26	29	0	0	NUM
ecletica-640	26	30	°	°	NOUN
ecletica-640	26	31	c	c	NOUN
ecletica-640	26	32	,	,	PUNCT
ecletica-640	26	33	were	be	AUX
ecletica-640	26	34	added	add	VERB
ecletica-640	26	35	20.0	20.0	NUM
ecletica-640	26	36	mmol	mmol	NOUN
ecletica-640	26	37	(	(	PUNCT
ecletica-640	26	38	8	8	NUM
ecletica-640	26	39	ml	ml	NOUN
ecletica-640	26	40	)	)	PUNCT
ecletica-640	26	41	of	of	ADP
ecletica-640	26	42	n	n	CCONJ
ecletica-640	26	43	-	-	PUNCT
ecletica-640	26	44	buli	buli	NOUN
ecletica-640	26	45	in	in	ADP
ecletica-640	26	46	hexane	hexane	NOUN
ecletica-640	26	47	.	.	PUNCT
ecletica-640	27	1	the	the	DET
ecletica-640	27	2	solution	solution	NOUN
ecletica-640	27	3	was	be	AUX
ecletica-640	27	4	cooled	cool	VERB
ecletica-640	27	5	to	to	ADP
ecletica-640	27	6	-78	-78	PROPN
ecletica-640	27	7	°	°	PROPN
ecletica-640	27	8	c	c	NOUN
ecletica-640	27	9	and	and	CCONJ
ecletica-640	27	10	10.0	10.0	NUM
ecletica-640	27	11	mmol	mmol	NOUN
ecletica-640	27	12	(	(	PUNCT
ecletica-640	27	13	1.14	1.14	NUM
ecletica-640	27	14	g	g	NOUN
ecletica-640	27	15	)	)	PUNCT
ecletica-640	27	16	of	of	ADP
ecletica-640	27	17	e	e	NOUN
ecletica-640	27	18	-	-	NOUN
ecletica-640	27	19	caprolactone	caprolactone	ADJ
ecletica-640	27	20	(	(	PUNCT
ecletica-640	27	21	10	10	NUM
ecletica-640	27	22	)	)	PUNCT
ecletica-640	27	23	were	be	AUX
ecletica-640	27	24	added	add	VERB
ecletica-640	27	25	followed	follow	VERB
ecletica-640	27	26	,	,	PUNCT
ecletica-640	27	27	after	after	ADP
ecletica-640	27	28	30	30	NUM
ecletica-640	27	29	min	min	NOUN
ecletica-640	27	30	.	.	PROPN
ecletica-640	27	31	,	,	PUNCT
ecletica-640	27	32	by	by	ADP
ecletica-640	27	33	10.0	10.0	NUM
ecletica-640	27	34	mmol	mmol	NOUN
ecletica-640	27	35	(	(	PUNCT
ecletica-640	27	36	0.8	0.8	NUM
ecletica-640	27	37	ml	ml	NOUN
ecletica-640	27	38	)	)	PUNCT
ecletica-640	27	39	of	of	ADP
ecletica-640	27	40	methyl	methyl	NOUN
ecletica-640	27	41	chloroformiate	chloroformiate	NOUN
ecletica-640	27	42	.	.	PUNCT
ecletica-640	28	1	after	after	ADP
ecletica-640	28	2	1	1	NUM
ecletica-640	28	3	h	h	NOUN
ecletica-640	28	4	at	at	ADP
ecletica-640	28	5	-78	-78	PROPN
ecletica-640	28	6	°	°	PROPN
ecletica-640	28	7	c	c	NOUN
ecletica-640	28	8	,	,	PUNCT
ecletica-640	28	9	the	the	DET
ecletica-640	28	10	temperature	temperature	NOUN
ecletica-640	28	11	was	be	AUX
ecletica-640	28	12	allowed	allow	VERB
ecletica-640	28	13	to	to	PART
ecletica-640	28	14	rise	rise	VERB
ecletica-640	28	15	to	to	ADP
ecletica-640	28	16	-30	-30	PROPN
ecletica-640	28	17	°	°	NOUN
ecletica-640	28	18	c	c	NOUN
ecletica-640	28	19	and	and	CCONJ
ecletica-640	28	20	quenched	quench	VERB
ecletica-640	28	21	with	with	ADP
ecletica-640	28	22	2	2	NUM
ecletica-640	28	23	ml	ml	NOUN
ecletica-640	28	24	of	of	ADP
ecletica-640	28	25	glacial	glacial	ADJ
ecletica-640	28	26	acetic	acetic	ADJ
ecletica-640	28	27	acid	acid	NOUN
ecletica-640	28	28	.	.	PUNCT
ecletica-640	29	1	the	the	DET
ecletica-640	29	2	solution	solution	NOUN
ecletica-640	29	3	was	be	AUX
ecletica-640	29	4	diluted	dilute	VERB
ecletica-640	29	5	with	with	ADP
ecletica-640	29	6	water	water	NOUN
ecletica-640	29	7	and	and	CCONJ
ecletica-640	29	8	extracted	extract	VERB
ecletica-640	29	9	with	with	ADP
ecletica-640	29	10	ch2cl2	ch2cl2	PUNCT
ecletica-640	29	11	(	(	PUNCT
ecletica-640	29	12	3	3	NUM
ecletica-640	29	13	x	x	SYM
ecletica-640	29	14	20	20	NUM
ecletica-640	29	15	ml	ml	NOUN
ecletica-640	29	16	)	)	PUNCT
ecletica-640	29	17	.	.	PUNCT
ecletica-640	30	1	the	the	DET
ecletica-640	30	2	combined	combine	VERB
ecletica-640	30	3	extracts	extract	NOUN
ecletica-640	30	4	were	be	AUX
ecletica-640	30	5	dried	dry	VERB
ecletica-640	30	6	over	over	ADP
ecletica-640	30	7	na2so4	na2so4	NOUN
ecletica-640	30	8	and	and	CCONJ
ecletica-640	30	9	evaporated	evaporate	VERB
ecletica-640	30	10	.	.	PUNCT
ecletica-640	31	1	the	the	DET
ecletica-640	31	2	oily	oily	ADJ
ecletica-640	31	3	residue	residue	NOUN
ecletica-640	31	4	was	be	AUX
ecletica-640	31	5	purified	purify	VERB
ecletica-640	31	6	over	over	ADP
ecletica-640	31	7	a	a	DET
ecletica-640	31	8	silica	silica	NOUN
ecletica-640	31	9	gel	gel	NOUN
ecletica-640	31	10	column	column	NOUN
ecletica-640	31	11	using	use	VERB
ecletica-640	31	12	toluene	toluene	NOUN
ecletica-640	31	13	containing	contain	VERB
ecletica-640	31	14	5	5	NUM
ecletica-640	31	15	-	-	SYM
ecletica-640	31	16	10	10	NUM
ecletica-640	31	17	%	%	NOUN
ecletica-640	31	18	of	of	ADP
ecletica-640	31	19	etoac	etoac	ADJ
ecletica-640	31	20	as	as	ADP
ecletica-640	31	21	eluent	eluent	NOUN
ecletica-640	31	22	.	.	PUNCT
ecletica-640	32	1	yield	yield	NOUN
ecletica-640	32	2	:	:	PUNCT
ecletica-640	32	3	0.318	0.318	NUM
ecletica-640	32	4	g	g	PROPN
ecletica-640	32	5	(	(	PUNCT
ecletica-640	32	6	18.5	18.5	NUM
ecletica-640	32	7	%	%	NOUN
ecletica-640	32	8	)	)	PUNCT
ecletica-640	32	9	of	of	ADP
ecletica-640	32	10	yellowish	yellowish	ADJ
ecletica-640	32	11	oil	oil	NOUN
ecletica-640	32	12	.	.	PUNCT
ecletica-640	33	1	nmr1h	nmr1h	PROPN
ecletica-640	34	1	(	(	PUNCT
ecletica-640	34	2	ccl4	ccl4	PROPN
ecletica-640	34	3	)	)	PUNCT
ecletica-640	35	1	d	d	NOUN
ecletica-640	35	2	:	:	PUNCT
ecletica-640	35	3	1.63	1.63	NUM
ecletica-640	35	4	-	-	SYM
ecletica-640	35	5	2.10	2.10	NUM
ecletica-640	35	6	(	(	PUNCT
ecletica-640	35	7	m	m	PROPN
ecletica-640	35	8	,	,	PUNCT
ecletica-640	35	9	6h	6h	NUM
ecletica-640	35	10	)	)	PUNCT
ecletica-640	35	11	;	;	PUNCT
ecletica-640	35	12	3.53	3.53	NUM
ecletica-640	35	13	-	-	SYM
ecletica-640	35	14	3.87	3.87	NUM
ecletica-640	35	15	(	(	PUNCT
ecletica-640	35	16	m	m	PROPN
ecletica-640	35	17	,	,	PUNCT
ecletica-640	35	18	superimposed	superimpose	VERB
ecletica-640	35	19	to	to	ADP
ecletica-640	35	20	3.77	3.77	NUM
ecletica-640	35	21	(	(	PUNCT
ecletica-640	35	22	s	s	NOUN
ecletica-640	35	23	)	)	PUNCT
ecletica-640	35	24	total	total	ADJ
ecletica-640	35	25	4h	4h	NUM
ecletica-640	35	26	)	)	PUNCT
ecletica-640	35	27	;	;	PUNCT
ecletica-640	35	28	4.17	4.17	NUM
ecletica-640	35	29	-	-	SYM
ecletica-640	35	30	4.43	4.43	NUM
ecletica-640	35	31	(	(	PUNCT
ecletica-640	35	32	m	m	PROPN
ecletica-640	35	33	,	,	PUNCT
ecletica-640	35	34	2h	2h	NUM
ecletica-640	35	35	)	)	PUNCT
ecletica-640	35	36	.	.	PUNCT
ecletica-640	36	1	2	2	NUM
ecletica-640	36	2	-	-	PUNCT
ecletica-640	36	3	trimethylsilyloxy-2	trimethylsilyloxy-2	NUM
ecletica-640	36	4	-	-	PUNCT
ecletica-640	36	5	oxepene	oxepene	NOUN
ecletica-640	36	6	(	(	PUNCT
ecletica-640	36	7	13	13	NUM
ecletica-640	36	8	):	):	PUNCT
ecletica-640	36	9	to	to	ADP
ecletica-640	36	10	a	a	DET
ecletica-640	36	11	solution	solution	NOUN
ecletica-640	36	12	of	of	ADP
ecletica-640	36	13	12.0	12.0	NUM
ecletica-640	36	14	mmol	mmol	NOUN
ecletica-640	36	15	of	of	ADP
ecletica-640	36	16	the	the	DET
ecletica-640	36	17	enolate	enolate	NOUN
ecletica-640	36	18	of	of	ADP
ecletica-640	36	19	(	(	PUNCT
ecletica-640	36	20	10	10	NUM
ecletica-640	36	21	)	)	PUNCT
ecletica-640	36	22	in	in	ADP
ecletica-640	36	23	10	10	NUM
ecletica-640	36	24	ml	ml	NOUN
ecletica-640	36	25	of	of	ADP
ecletica-640	36	26	thf	thf	NOUN
ecletica-640	36	27	,	,	PUNCT
ecletica-640	36	28	prepared	prepare	VERB
ecletica-640	36	29	as	as	SCONJ
ecletica-640	36	30	described	describe	VERB
ecletica-640	36	31	before	before	ADV
ecletica-640	36	32	,	,	PUNCT
ecletica-640	36	33	were	be	AUX
ecletica-640	36	34	added	add	VERB
ecletica-640	36	35	12.0	12.0	NUM
ecletica-640	36	36	mmol	mmol	NOUN
ecletica-640	36	37	(	(	PUNCT
ecletica-640	36	38	1.5	1.5	NUM
ecletica-640	36	39	ml	ml	NOUN
ecletica-640	36	40	)	)	PUNCT
ecletica-640	36	41	of	of	ADP
ecletica-640	36	42	chlorotrimethylsilane	chlorotrimethylsilane	NOUN
ecletica-640	36	43	at	at	ADP
ecletica-640	36	44	-78	-78	PROPN
ecletica-640	36	45	°	°	PROPN
ecletica-640	36	46	c.	c.	NOUN
ecletica-640	36	47	the	the	DET
ecletica-640	36	48	mixture	mixture	NOUN
ecletica-640	36	49	was	be	AUX
ecletica-640	36	50	allowed	allow	VERB
ecletica-640	36	51	to	to	PART
ecletica-640	36	52	warm	warm	VERB
ecletica-640	36	53	to	to	ADP
ecletica-640	36	54	0	0	NUM
ecletica-640	36	55	°	°	NOUN
ecletica-640	37	1	c	c	X
ecletica-640	37	2	,	,	PUNCT
ecletica-640	37	3	hydrolyzed	hydrolyze	VERB
ecletica-640	37	4	with	with	ADP
ecletica-640	37	5	100	100	NUM
ecletica-640	37	6	g	g	NOUN
ecletica-640	37	7	of	of	ADP
ecletica-640	37	8	crushed	crushed	ADJ
ecletica-640	37	9	ice	ice	NOUN
ecletica-640	37	10	and	and	CCONJ
ecletica-640	37	11	extracted	extract	VERB
ecletica-640	37	12	with	with	ADP
ecletica-640	37	13	hexane	hexane	NOUN
ecletica-640	37	14	(	(	PUNCT
ecletica-640	37	15	3	3	NUM
ecletica-640	37	16	x	x	SYM
ecletica-640	37	17	20	20	NUM
ecletica-640	37	18	ml	ml	NOUN
ecletica-640	37	19	)	)	PUNCT
ecletica-640	37	20	.	.	PUNCT
ecletica-640	38	1	the	the	DET
ecletica-640	38	2	combinade	combinade	ADJ
ecletica-640	38	3	extracts	extract	NOUN
ecletica-640	38	4	were	be	AUX
ecletica-640	38	5	washed	wash	VERB
ecletica-640	38	6	with	with	ADP
ecletica-640	38	7	water	water	NOUN
ecletica-640	38	8	and	and	CCONJ
ecletica-640	38	9	dried	dry	VERB
ecletica-640	38	10	over	over	ADP
ecletica-640	38	11	k2co3	k2co3	ADJ
ecletica-640	38	12	.	.	PUNCT
ecletica-640	39	1	after	after	ADP
ecletica-640	39	2	evaporation	evaporation	NOUN
ecletica-640	39	3	of	of	ADP
ecletica-640	39	4	the	the	DET
ecletica-640	39	5	solvent	solvent	NOUN
ecletica-640	39	6	,	,	PUNCT
ecletica-640	39	7	the	the	DET
ecletica-640	39	8	product	product	NOUN
ecletica-640	39	9	was	be	AUX
ecletica-640	39	10	distilled	distil	VERB
ecletica-640	39	11	in	in	ADP
ecletica-640	39	12	vacuo	vacuo	PROPN
ecletica-640	39	13	.	.	PUNCT
ecletica-640	40	1	yield	yield	NOUN
ecletica-640	40	2	:	:	PUNCT
ecletica-640	40	3	0.649	0.649	NUM
ecletica-640	40	4	g	g	NOUN
ecletica-640	40	5	(	(	PUNCT
ecletica-640	40	6	34.9	34.9	NUM
ecletica-640	40	7	%	%	NOUN
ecletica-640	40	8	)	)	PUNCT
ecletica-640	40	9	of	of	ADP
ecletica-640	40	10	colourless	colourless	ADJ
ecletica-640	40	11	liquid	liquid	NOUN
ecletica-640	40	12	,	,	PUNCT
ecletica-640	40	13	b.p	b.p	PROPN
ecletica-640	40	14	.	.	PROPN
ecletica-640	40	15	65	65	NUM
ecletica-640	40	16	-	-	SYM
ecletica-640	40	17	67	67	NUM
ecletica-640	40	18	°	°	NUM
ecletica-640	41	1	c	c	NOUN
ecletica-640	41	2	(	(	PUNCT
ecletica-640	41	3	1	1	NUM
ecletica-640	41	4	mm	mm	NOUN
ecletica-640	41	5	)	)	PUNCT
ecletica-640	41	6	.	.	PUNCT
ecletica-640	42	1	nmr1h	nmr1h	PROPN
ecletica-640	42	2	(	(	PUNCT
ecletica-640	42	3	ccl4	ccl4	PROPN
ecletica-640	42	4	)	)	PUNCT
ecletica-640	43	1	d	d	NOUN
ecletica-640	43	2	:	:	PUNCT
ecletica-640	43	3	0.62	0.62	NUM
ecletica-640	43	4	(	(	PUNCT
ecletica-640	43	5	s	s	PROPN
ecletica-640	43	6	,	,	PUNCT
ecletica-640	43	7	9h	9h	NUM
ecletica-640	43	8	)	)	PUNCT
ecletica-640	43	9	;	;	PUNCT
ecletica-640	43	10	1.83	1.83	NUM
ecletica-640	43	11	-	-	SYM
ecletica-640	43	12	2.77	2.77	NUM
ecletica-640	43	13	(	(	PUNCT
ecletica-640	43	14	m	m	PROPN
ecletica-640	43	15	,	,	PUNCT
ecletica-640	43	16	6h	6h	NUM
ecletica-640	43	17	)	)	PUNCT
ecletica-640	43	18	;	;	PUNCT
ecletica-640	43	19	4.00	4.00	NUM
ecletica-640	43	20	-	-	SYM
ecletica-640	43	21	4.23	4.23	NUM
ecletica-640	43	22	(	(	PUNCT
ecletica-640	43	23	m	m	PROPN
ecletica-640	43	24	,	,	PUNCT
ecletica-640	43	25	3h	3h	NUM
ecletica-640	43	26	)	)	PUNCT
ecletica-640	43	27	.	.	PUNCT
ecletica-640	44	1	3	3	X
ecletica-640	44	2	-	-	PUNCT
ecletica-640	44	3	allyl-2	allyl-2	VERB
ecletica-640	44	4	-	-	PUNCT
ecletica-640	44	5	oxepanone	oxepanone	NOUN
ecletica-640	44	6	(	(	PUNCT
ecletica-640	44	7	15	15	NUM
ecletica-640	44	8	):	):	PUNCT
ecletica-640	44	9	to	to	ADP
ecletica-640	44	10	a	a	DET
ecletica-640	44	11	solution	solution	NOUN
ecletica-640	44	12	of	of	ADP
ecletica-640	44	13	15.0	15.0	NUM
ecletica-640	44	14	mmol	mmol	NOUN
ecletica-640	44	15	of	of	ADP
ecletica-640	44	16	the	the	DET
ecletica-640	44	17	enolate	enolate	NOUN
ecletica-640	44	18	of	of	ADP
ecletica-640	44	19	(	(	PUNCT
ecletica-640	44	20	10	10	NUM
ecletica-640	44	21	)	)	PUNCT
ecletica-640	44	22	in	in	ADP
ecletica-640	44	23	15	15	NUM
ecletica-640	44	24	ml	ml	NOUN
ecletica-640	44	25	of	of	ADP
ecletica-640	44	26	thf	thf	NOUN
ecletica-640	44	27	,	,	PUNCT
ecletica-640	44	28	prepared	prepare	VERB
ecletica-640	44	29	as	as	SCONJ
ecletica-640	44	30	described	describe	VERB
ecletica-640	44	31	for	for	ADP
ecletica-640	44	32	(	(	PUNCT
ecletica-640	44	33	12	12	NUM
ecletica-640	44	34	)	)	PUNCT
ecletica-640	44	35	,	,	PUNCT
ecletica-640	44	36	were	be	AUX
ecletica-640	44	37	added	add	VERB
ecletica-640	44	38	15.0	15.0	NUM
ecletica-640	44	39	mmol	mmol	NOUN
ecletica-640	44	40	(	(	PUNCT
ecletica-640	44	41	1.4	1.4	NUM
ecletica-640	44	42	ml	ml	NOUN
ecletica-640	44	43	)	)	PUNCT
ecletica-640	44	44	of	of	ADP
ecletica-640	44	45	allyl	allyl	ADJ
ecletica-640	44	46	iodide	iodide	NOUN
ecletica-640	44	47	at	at	ADP
ecletica-640	44	48	-78	-78	PROPN
ecletica-640	44	49	°	°	PROPN
ecletica-640	44	50	c.	c.	NOUN
ecletica-640	44	51	after	after	ADP
ecletica-640	44	52	1	1	NUM
ecletica-640	44	53	h	h	NOUN
ecletica-640	44	54	at	at	ADP
ecletica-640	44	55	this	this	DET
ecletica-640	44	56	temperature	temperature	NOUN
ecletica-640	44	57	,	,	PUNCT
ecletica-640	44	58	the	the	DET
ecletica-640	44	59	solution	solution	NOUN
ecletica-640	44	60	was	be	AUX
ecletica-640	44	61	allowed	allow	VERB
ecletica-640	44	62	to	to	PART
ecletica-640	44	63	warm	warm	VERB
ecletica-640	44	64	up	up	ADP
ecletica-640	44	65	to	to	ADP
ecletica-640	44	66	-30	-30	PROPN
ecletica-640	44	67	°	°	NOUN
ecletica-640	44	68	c	c	NOUN
ecletica-640	44	69	and	and	CCONJ
ecletica-640	44	70	quenched	quench	VERB
ecletica-640	44	71	with	with	ADP
ecletica-640	44	72	1	1	NUM
ecletica-640	44	73	ml	ml	NOUN
ecletica-640	44	74	of	of	ADP
ecletica-640	44	75	glacial	glacial	ADJ
ecletica-640	44	76	acetic	acetic	ADJ
ecletica-640	44	77	acid	acid	NOUN
ecletica-640	44	78	.	.	PUNCT
ecletica-640	45	1	the	the	DET
ecletica-640	45	2	mixture	mixture	NOUN
ecletica-640	45	3	was	be	AUX
ecletica-640	45	4	diluted	dilute	VERB
ecletica-640	45	5	with	with	ADP
ecletica-640	45	6	water	water	NOUN
ecletica-640	45	7	and	and	CCONJ
ecletica-640	45	8	extracted	extract	VERB
ecletica-640	45	9	with	with	ADP
ecletica-640	45	10	ch2cl2	ch2cl2	PUNCT
ecletica-640	45	11	(	(	PUNCT
ecletica-640	45	12	3	3	NUM
ecletica-640	45	13	x	x	SYM
ecletica-640	45	14	20	20	NUM
ecletica-640	45	15	ml	ml	NOUN
ecletica-640	45	16	)	)	PUNCT
ecletica-640	45	17	.	.	PUNCT
ecletica-640	46	1	the	the	DET
ecletica-640	46	2	combinade	combinade	ADJ
ecletica-640	46	3	extracts	extract	NOUN
ecletica-640	46	4	were	be	AUX
ecletica-640	46	5	washed	wash	VERB
ecletica-640	46	6	with	with	ADP
ecletica-640	46	7	nahco3	nahco3	ADJ
ecletica-640	46	8	solution	solution	NOUN
ecletica-640	46	9	and	and	CCONJ
ecletica-640	46	10	water	water	NOUN
ecletica-640	46	11	,	,	PUNCT
ecletica-640	46	12	dried	dry	VERB
ecletica-640	46	13	over	over	ADP
ecletica-640	46	14	na2so4	na2so4	NOUN
ecletica-640	46	15	and	and	CCONJ
ecletica-640	46	16	evaporated	evaporate	VERB
ecletica-640	46	17	.	.	PUNCT
ecletica-640	47	1	flash	flash	VERB
ecletica-640	47	2	distillation	distillation	NOUN
ecletica-640	47	3	of	of	ADP
ecletica-640	47	4	the	the	DET
ecletica-640	47	5	remaining	remain	VERB
ecletica-640	47	6	oil	oil	NOUN
ecletica-640	47	7	yielded	yield	VERB
ecletica-640	47	8	0.679	0.679	NUM
ecletica-640	47	9	g	g	NOUN
ecletica-640	47	10	(	(	PUNCT
ecletica-640	47	11	26.6	26.6	NUM
ecletica-640	47	12	%	%	NOUN
ecletica-640	47	13	)	)	PUNCT
ecletica-640	47	14	of	of	ADP
ecletica-640	47	15	colourless	colourless	ADJ
ecletica-640	47	16	oil	oil	NOUN
ecletica-640	47	17	,	,	PUNCT
ecletica-640	47	18	b.p	b.p	PROPN
ecletica-640	47	19	.	.	PROPN
ecletica-640	47	20	115	115	NUM
ecletica-640	47	21	-	-	SYM
ecletica-640	47	22	117	117	NUM
ecletica-640	47	23	°	°	ADP
ecletica-640	47	24	c	c	NOUN
ecletica-640	47	25	(	(	PUNCT
ecletica-640	47	26	1	1	NUM
ecletica-640	47	27	mm	mm	NOUN
ecletica-640	47	28	)	)	PUNCT
ecletica-640	47	29	.	.	PUNCT
ecletica-640	48	1	nmr1h	nmr1h	PROPN
ecletica-640	48	2	(	(	PUNCT
ecletica-640	48	3	ccl4	ccl4	PROPN
ecletica-640	48	4	)	)	PUNCT
ecletica-640	49	1	d	d	NOUN
ecletica-640	49	2	:	:	PUNCT
ecletica-640	49	3	1.13	1.13	NUM
ecletica-640	49	4	-	-	SYM
ecletica-640	49	5	2.03	2.03	NUM
ecletica-640	49	6	(	(	PUNCT
ecletica-640	49	7	m	m	PROPN
ecletica-640	49	8	,	,	PUNCT
ecletica-640	49	9	7h	7h	PROPN
ecletica-640	49	10	)	)	PUNCT
ecletica-640	49	11	;	;	PUNCT
ecletica-640	49	12	2.30	2.30	NUM
ecletica-640	49	13	-	-	SYM
ecletica-640	49	14	2.80	2.80	NUM
ecletica-640	49	15	(	(	PUNCT
ecletica-640	49	16	m	m	PROPN
ecletica-640	49	17	,	,	PUNCT
ecletica-640	49	18	2h	2h	NUM
ecletica-640	49	19	)	)	PUNCT
ecletica-640	49	20	;	;	PUNCT
ecletica-640	49	21	4.20	4.20	NUM
ecletica-640	49	22	(	(	PUNCT
ecletica-640	49	23	m	m	PROPN
ecletica-640	49	24	,	,	PUNCT
ecletica-640	49	25	2h	2h	NUM
ecletica-640	49	26	)	)	PUNCT
ecletica-640	49	27	;	;	PUNCT
ecletica-640	49	28	4.93	4.93	NUM
ecletica-640	49	29	-	-	SYM
ecletica-640	49	30	5.27	5.27	NUM
ecletica-640	49	31	(	(	PUNCT
ecletica-640	49	32	m	m	PROPN
ecletica-640	49	33	,	,	PUNCT
ecletica-640	49	34	2h	2h	NUM
ecletica-640	49	35	)	)	PUNCT
ecletica-640	49	36	;	;	PUNCT
ecletica-640	49	37	5.53	5.53	NUM
ecletica-640	49	38	-	-	SYM
ecletica-640	49	39	6.10	6.10	NUM
ecletica-640	49	40	(	(	PUNCT
ecletica-640	49	41	m	m	PROPN
ecletica-640	49	42	,	,	PUNCT
ecletica-640	49	43	1h	1h	NUM
ecletica-640	49	44	)	)	PUNCT
ecletica-640	49	45	.	.	PUNCT
ecletica-640	50	1	3,7	3,7	NUM
ecletica-640	50	2	-	-	PUNCT
ecletica-640	50	3	dimethyl-6-[2-(2	dimethyl-6-[2-(2	ADJ
ecletica-640	50	4	-	-	PUNCT
ecletica-640	50	5	naphthyl)ethyl]octane-1,7	naphthyl)ethyl]octane-1,7	NOUN
ecletica-640	50	6	-	-	PUNCT
ecletica-640	50	7	diol	diol	NOUN
ecletica-640	50	8	(	(	PUNCT
ecletica-640	50	9	18	18	NUM
ecletica-640	50	10	):	):	PUNCT
ecletica-640	50	11	to	to	ADP
ecletica-640	50	12	a	a	DET
ecletica-640	50	13	solution	solution	NOUN
ecletica-640	50	14	of	of	ADP
ecletica-640	50	15	1.0	1.0	NUM
ecletica-640	50	16	mmol	mmol	NOUN
ecletica-640	50	17	(	(	PUNCT
ecletica-640	50	18	0.282	0.282	NUM
ecletica-640	50	19	g	g	NOUN
ecletica-640	50	20	)	)	PUNCT
ecletica-640	50	21	of	of	ADP
ecletica-640	50	22	(	(	PUNCT
ecletica-640	50	23	6	6	NUM
ecletica-640	50	24	)	)	PUNCT
ecletica-640	50	25	(	(	PUNCT
ecletica-640	50	26	x	x	X
ecletica-640	50	27	=	=	PUNCT
ecletica-640	50	28	i	i	PROPN
ecletica-640	50	29	)	)	PUNCT
ecletica-640	50	30	in	in	ADP
ecletica-640	50	31	5	5	NUM
ecletica-640	50	32	ml	ml	NOUN
ecletica-640	50	33	of	of	ADP
ecletica-640	50	34	thf	thf	NOUN
ecletica-640	50	35	was	be	AUX
ecletica-640	50	36	added	add	VERB
ecletica-640	50	37	,	,	PUNCT
ecletica-640	50	38	at	at	ADP
ecletica-640	50	39	room	room	NOUN
ecletica-640	50	40	temperature	temperature	NOUN
ecletica-640	50	41	,	,	PUNCT
ecletica-640	50	42	an	an	DET
ecletica-640	50	43	excess	excess	NOUN
ecletica-640	50	44	of	of	ADP
ecletica-640	50	45	metallic	metallic	ADJ
ecletica-640	50	46	lithium	lithium	NOUN
ecletica-640	50	47	.	.	PUNCT
ecletica-640	51	1	the	the	DET
ecletica-640	51	2	reaction	reaction	NOUN
ecletica-640	51	3	was	be	AUX
ecletica-640	51	4	started	start	VERB
ecletica-640	51	5	by	by	ADP
ecletica-640	51	6	sonication	sonication	NOUN
ecletica-640	51	7	for	for	ADP
ecletica-640	51	8	2	2	NUM
ecletica-640	51	9	min	min	NOUN
ecletica-640	51	10	and	and	CCONJ
ecletica-640	51	11	then	then	ADV
ecletica-640	51	12	stirred	stir	VERB
ecletica-640	51	13	for	for	ADP
ecletica-640	51	14	3	3	NUM
ecletica-640	51	15	h	h	NOUN
ecletica-640	51	16	at	at	ADP
ecletica-640	51	17	0	0	NUM
ecletica-640	51	18	°	°	PROPN
ecletica-640	51	19	c.	c.	NOUN
ecletica-640	51	20	during	during	ADP
ecletica-640	51	21	this	this	DET
ecletica-640	51	22	time	time	NOUN
ecletica-640	51	23	,	,	PUNCT
ecletica-640	51	24	0.5	0.5	NUM
ecletica-640	51	25	mmol	mmol	NOUN
ecletica-640	51	26	(	(	PUNCT
ecletica-640	51	27	0.095	0.095	NUM
ecletica-640	51	28	g	g	NOUN
ecletica-640	51	29	)	)	PUNCT
ecletica-640	51	30	of	of	ADP
ecletica-640	51	31	cooper	cooper	NOUN
ecletica-640	51	32	(	(	PUNCT
ecletica-640	51	33	i	i	NOUN
ecletica-640	51	34	)	)	PUNCT
ecletica-640	51	35	iodide	iodide	NOUN
ecletica-640	51	36	were	be	AUX
ecletica-640	51	37	suspended	suspend	VERB
ecletica-640	51	38	in	in	ADP
ecletica-640	51	39	2	2	NUM
ecletica-640	51	40	ml	ml	NOUN
ecletica-640	51	41	of	of	ADP
ecletica-640	51	42	thf	thf	NOUN
ecletica-640	51	43	and	and	CCONJ
ecletica-640	51	44	0.25	0.25	NUM
ecletica-640	51	45	mmol	mmol	NOUN
ecletica-640	51	46	(	(	PUNCT
ecletica-640	51	47	0.040	0.040	NUM
ecletica-640	51	48	g	g	NOUN
ecletica-640	51	49	)	)	PUNCT
ecletica-640	51	50	of	of	ADP
ecletica-640	51	51	epoxycitronellol	epoxycitronellol	NOUN
ecletica-640	51	52	(	(	PUNCT
ecletica-640	51	53	17	17	NUM
ecletica-640	51	54	)	)	PUNCT
ecletica-640	51	55	and	and	CCONJ
ecletica-640	51	56	0.25	0.25	NUM
ecletica-640	51	57	mmol	mmol	NOUN
ecletica-640	51	58	(	(	PUNCT
ecletica-640	51	59	0.1	0.1	NUM
ecletica-640	51	60	ml	ml	NOUN
ecletica-640	51	61	)	)	PUNCT
ecletica-640	51	62	of	of	ADP
ecletica-640	51	63	n	n	CCONJ
ecletica-640	51	64	-	-	PUNCT
ecletica-640	51	65	buli	buli	PROPN
ecletica-640	51	66	were	be	AUX
ecletica-640	51	67	added	add	VERB
ecletica-640	51	68	at	at	ADP
ecletica-640	51	69	-50	-50	PROPN
ecletica-640	51	70	°	°	PROPN
ecletica-640	51	71	c.	c.	NOUN
ecletica-640	51	72	after	after	ADP
ecletica-640	51	73	10	10	NUM
ecletica-640	51	74	min	min	NOUN
ecletica-640	51	75	.	.	PROPN
ecletica-640	51	76	,	,	PUNCT
ecletica-640	51	77	at	at	ADP
ecletica-640	51	78	-50	-50	PROPN
ecletica-640	51	79	°	°	PROPN
ecletica-640	51	80	c	c	X
ecletica-640	51	81	,	,	PUNCT
ecletica-640	51	82	the	the	DET
ecletica-640	51	83	lithium	lithium	NOUN
ecletica-640	51	84	reagent	reagent	NOUN
ecletica-640	51	85	prepared	prepare	VERB
ecletica-640	51	86	previously	previously	ADV
ecletica-640	51	87	was	be	AUX
ecletica-640	51	88	added	add	VERB
ecletica-640	51	89	by	by	ADP
ecletica-640	51	90	means	mean	NOUN
ecletica-640	51	91	of	of	ADP
ecletica-640	51	92	a	a	DET
ecletica-640	51	93	syringe	syringe	NOUN
ecletica-640	51	94	,	,	PUNCT
ecletica-640	51	95	avoiding	avoid	VERB
ecletica-640	51	96	the	the	DET
ecletica-640	51	97	excess	excess	NOUN
ecletica-640	51	98	of	of	ADP
ecletica-640	51	99	unreacted	unreacted	ADJ
ecletica-640	51	100	lithium	lithium	NOUN
ecletica-640	51	101	metal	metal	NOUN
ecletica-640	51	102	.	.	PUNCT
ecletica-640	52	1	on	on	ADP
ecletica-640	52	2	rising	rise	VERB
ecletica-640	52	3	the	the	DET
ecletica-640	52	4	temperature	temperature	NOUN
ecletica-640	52	5	slowly	slowly	ADV
ecletica-640	52	6	to	to	ADP
ecletica-640	52	7	-10	-10	NOUN
ecletica-640	52	8	°	°	NOUN
ecletica-640	52	9	c	c	X
ecletica-640	52	10	,	,	PUNCT
ecletica-640	52	11	a	a	DET
ecletica-640	52	12	green	green	ADJ
ecletica-640	52	13	,	,	PUNCT
ecletica-640	52	14	homogeneous	homogeneous	ADJ
ecletica-640	52	15	solution	solution	NOUN
ecletica-640	52	16	was	be	AUX
ecletica-640	52	17	formed	form	VERB
ecletica-640	52	18	which	which	PRON
ecletica-640	52	19	was	be	AUX
ecletica-640	52	20	kept	keep	VERB
ecletica-640	52	21	for	for	ADP
ecletica-640	52	22	2	2	NUM
ecletica-640	52	23	days	day	NOUN
ecletica-640	52	24	at	at	ADP
ecletica-640	52	25	-7	-7	PROPN
ecletica-640	52	26	°	°	PROPN
ecletica-640	52	27	c.	c.	NOUN
ecletica-640	52	28	the	the	DET
ecletica-640	52	29	reaction	reaction	NOUN
ecletica-640	52	30	was	be	AUX
ecletica-640	52	31	hydrolyzed	hydrolyze	VERB
ecletica-640	52	32	with	with	ADP
ecletica-640	52	33	saturated	saturate	VERB
ecletica-640	52	34	nh4cl	nh4cl	NUM
ecletica-640	52	35	solution	solution	NOUN
ecletica-640	52	36	and	and	CCONJ
ecletica-640	52	37	extracted	extract	VERB
ecletica-640	52	38	with	with	ADP
ecletica-640	52	39	ch2cl2	ch2cl2	PUNCT
ecletica-640	52	40	(	(	PUNCT
ecletica-640	52	41	3	3	NUM
ecletica-640	52	42	x	x	SYM
ecletica-640	52	43	20	20	NUM
ecletica-640	52	44	ml	ml	NOUN
ecletica-640	52	45	)	)	PUNCT
ecletica-640	52	46	.	.	PUNCT
ecletica-640	53	1	after	after	ADP
ecletica-640	53	2	drying	dry	VERB
ecletica-640	53	3	over	over	ADP
ecletica-640	53	4	na2so4	na2so4	NOUN
ecletica-640	53	5	and	and	CCONJ
ecletica-640	53	6	evaporation	evaporation	NOUN
ecletica-640	53	7	,	,	PUNCT
ecletica-640	53	8	the	the	DET
ecletica-640	53	9	crystalline	crystalline	ADJ
ecletica-640	53	10	residue	residue	NOUN
ecletica-640	53	11	was	be	AUX
ecletica-640	53	12	purified	purify	VERB
ecletica-640	53	13	on	on	ADP
ecletica-640	53	14	a	a	DET
ecletica-640	53	15	silica	silica	NOUN
ecletica-640	53	16	gel	gel	NOUN
ecletica-640	53	17	column	column	NOUN
ecletica-640	53	18	eluting	elute	VERB
ecletica-640	53	19	initially	initially	ADV
ecletica-640	53	20	with	with	ADP
ecletica-640	53	21	pure	pure	ADJ
ecletica-640	53	22	cyclohexane	cyclohexane	NOUN
ecletica-640	53	23	,	,	PUNCT
ecletica-640	53	24	then	then	ADV
ecletica-640	53	25	cyclohexane	cyclohexane	NOUN
ecletica-640	53	26	/	/	SYM
ecletica-640	53	27	toluene	toluene	NOUN
ecletica-640	53	28	mixtures	mixture	NOUN
ecletica-640	53	29	and	and	CCONJ
ecletica-640	53	30	at	at	ADP
ecletica-640	53	31	least	least	ADJ
ecletica-640	53	32	pure	pure	ADJ
ecletica-640	53	33	toluene	toluene	NOUN
ecletica-640	53	34	.	.	PUNCT
ecletica-640	54	1	the	the	DET
ecletica-640	54	2	less	less	ADV
ecletica-640	54	3	polar	polar	ADJ
ecletica-640	54	4	fractions	fraction	NOUN
ecletica-640	54	5	yielded	yield	VERB
ecletica-640	54	6	0,097	0,097	NUM
ecletica-640	54	7	g	g	NOUN
ecletica-640	54	8	of	of	ADP
ecletica-640	54	9	1,4	1,4	NOUN
ecletica-640	54	10	-	-	PUNCT
ecletica-640	54	11	di-2	di-2	NOUN
ecletica-640	54	12	-	-	PUNCT
ecletica-640	54	13	naphthylbutane	naphthylbutane	NOUN
ecletica-640	54	14	as	as	ADP
ecletica-640	54	15	colourless	colourless	ADJ
ecletica-640	54	16	needles	needle	NOUN
ecletica-640	54	17	,	,	PUNCT
ecletica-640	54	18	m.p	m.p	PROPN
ecletica-640	54	19	.	.	PROPN
ecletica-640	54	20	153	153	NUM
ecletica-640	54	21	-	-	SYM
ecletica-640	54	22	154	154	NUM
ecletica-640	54	23	°	°	NUM
ecletica-640	54	24	c	c	NOUN
ecletica-640	54	25	(	(	PUNCT
ecletica-640	54	26	lit.5	lit.5	NOUN
ecletica-640	54	27	:	:	PUNCT
ecletica-640	54	28	155	155	NUM
ecletica-640	54	29	-	-	SYM
ecletica-640	54	30	156	156	NUM
ecletica-640	54	31	°	°	NOUN
ecletica-640	54	32	c	c	NOUN
ecletica-640	54	33	)	)	PUNCT
ecletica-640	54	34	.	.	PUNCT
ecletica-640	55	1	the	the	DET
ecletica-640	55	2	toluene	toluene	NOUN
ecletica-640	55	3	fractions	fraction	NOUN
ecletica-640	55	4	yielded	yield	VERB
ecletica-640	55	5	0,047	0,047	NUM
ecletica-640	55	6	g	g	NOUN
ecletica-640	55	7	(	(	PUNCT
ecletica-640	55	8	57.3	57.3	NUM
ecletica-640	55	9	%	%	NOUN
ecletica-640	55	10	based	base	VERB
ecletica-640	55	11	on	on	ADP
ecletica-640	55	12	(	(	PUNCT
ecletica-640	55	13	17	17	NUM
ecletica-640	55	14	)	)	PUNCT
ecletica-640	55	15	)	)	PUNCT
ecletica-640	55	16	of	of	ADP
ecletica-640	55	17	diol	diol	NOUN
ecletica-640	55	18	(	(	PUNCT
ecletica-640	55	19	18	18	NUM
ecletica-640	55	20	)	)	PUNCT
ecletica-640	55	21	as	as	ADP
ecletica-640	55	22	colourless	colourless	ADJ
ecletica-640	55	23	prisms	prism	NOUN
ecletica-640	55	24	,	,	PUNCT
ecletica-640	55	25	m.p	m.p	PROPN
ecletica-640	55	26	.	.	PROPN
ecletica-640	55	27	60	60	NUM
ecletica-640	55	28	-	-	SYM
ecletica-640	55	29	61	61	NUM
ecletica-640	55	30	°	°	ADP
ecletica-640	55	31	c.	c.	PROPN
ecletica-640	55	32	nmr1h	nmr1h	PROPN
ecletica-640	56	1	(	(	PUNCT
ecletica-640	56	2	cdcl3	cdcl3	PROPN
ecletica-640	56	3	)	)	PUNCT
ecletica-640	57	1	d	d	NOUN
ecletica-640	57	2	:	:	PUNCT
ecletica-640	57	3	0.90	0.90	NUM
ecletica-640	57	4	(	(	PUNCT
ecletica-640	57	5	d	d	PROPN
ecletica-640	57	6	,	,	PUNCT
ecletica-640	57	7	3h	3h	NUM
ecletica-640	57	8	,	,	PUNCT
ecletica-640	57	9	j=6hz	j=6hz	X
ecletica-640	57	10	)	)	PUNCT
ecletica-640	57	11	;	;	PUNCT
ecletica-640	57	12	1.21	1.21	NUM
ecletica-640	57	13	(	(	PUNCT
ecletica-640	57	14	s	s	PROPN
ecletica-640	57	15	,	,	PUNCT
ecletica-640	57	16	3h	3h	NUM
ecletica-640	57	17	)	)	PUNCT
ecletica-640	57	18	;	;	PUNCT
ecletica-640	57	19	1.24	1.24	NUM
ecletica-640	57	20	(	(	PUNCT
ecletica-640	57	21	s	s	PROPN
ecletica-640	57	22	,	,	PUNCT
ecletica-640	57	23	3h	3h	NUM
ecletica-640	57	24	)	)	PUNCT
ecletica-640	57	25	;	;	PUNCT
ecletica-640	58	1	1.36	1.36	NUM
ecletica-640	58	2	-	-	SYM
ecletica-640	58	3	1.83	1.83	NUM
ecletica-640	58	4	(	(	PUNCT
ecletica-640	58	5	m	m	PROPN
ecletica-640	58	6	,	,	PUNCT
ecletica-640	58	7	12h	12h	NUM
ecletica-640	58	8	)	)	PUNCT
ecletica-640	58	9	;	;	PUNCT
ecletica-640	58	10	2.60	2.60	NUM
ecletica-640	58	11	-	-	SYM
ecletica-640	58	12	2.97	2.97	NUM
ecletica-640	58	13	(	(	PUNCT
ecletica-640	58	14	m	m	PROPN
ecletica-640	58	15	,	,	PUNCT
ecletica-640	58	16	2h	2h	NUM
ecletica-640	58	17	)	)	PUNCT
ecletica-640	58	18	;	;	PUNCT
ecletica-640	58	19	3.67	3.67	NUM
ecletica-640	58	20	(	(	PUNCT
ecletica-640	58	21	t	t	PROPN
ecletica-640	58	22	,	,	PUNCT
ecletica-640	58	23	2h	2h	NUM
ecletica-640	58	24	,	,	PUNCT
ecletica-640	58	25	j=6hz	j=6hz	X
ecletica-640	58	26	)	)	PUNCT
ecletica-640	58	27	;	;	PUNCT
ecletica-640	58	28	7.27	7.27	NUM
ecletica-640	58	29	-	-	SYM
ecletica-640	58	30	7.97	7.97	NUM
ecletica-640	58	31	(	(	PUNCT
ecletica-640	58	32	m	m	PROPN
ecletica-640	58	33	,	,	PUNCT
ecletica-640	58	34	7h	7h	NUM
ecletica-640	58	35	)	)	PUNCT
ecletica-640	58	36	.	.	PUNCT
ecletica-640	59	1	ir	ir	PROPN
ecletica-640	59	2	(	(	PUNCT
ecletica-640	59	3	kbr	kbr	PROPN
ecletica-640	59	4	)	)	PUNCT
ecletica-640	59	5	cm	cm	NOUN
ecletica-640	59	6	–	–	PUNCT
ecletica-640	59	7	1	1	NUM
ecletica-640	59	8	:	:	SYM
ecletica-640	59	9	3379	3379	NUM
ecletica-640	59	10	;	;	PUNCT
ecletica-640	59	11	3051	3051	NUM
ecletica-640	59	12	;	;	PUNCT
ecletica-640	59	13	2925	2925	NUM
ecletica-640	59	14	;	;	PUNCT
ecletica-640	59	15	1631	1631	NUM
ecletica-640	59	16	;	;	PUNCT
ecletica-640	59	17	1600	1600	NUM
ecletica-640	59	18	;	;	PUNCT
ecletica-640	59	19	1053	1053	NUM
ecletica-640	59	20	;	;	PUNCT
ecletica-640	59	21	790	790	NUM
ecletica-640	59	22	;	;	PUNCT
ecletica-640	59	23	750	750	NUM
ecletica-640	59	24	.	.	PUNCT
ecletica-640	59	25	results	result	NOUN
ecletica-640	59	26	and	and	CCONJ
ecletica-640	59	27	discussion	discussion	NOUN
ecletica-640	59	28	because	because	SCONJ
ecletica-640	59	29	of	of	ADP
ecletica-640	59	30	the	the	DET
ecletica-640	59	31	difficult	difficult	ADJ
ecletica-640	59	32	obtention	obtention	NOUN
ecletica-640	59	33	of	of	ADP
ecletica-640	59	34	both	both	DET
ecletica-640	59	35	starting	start	VERB
ecletica-640	59	36	materials	material	NOUN
ecletica-640	59	37	,	,	PUNCT
ecletica-640	59	38	(	(	PUNCT
ecletica-640	59	39	5	5	NUM
ecletica-640	59	40	)	)	PUNCT
ecletica-640	59	41	and	and	CCONJ
ecletica-640	59	42	(	(	PUNCT
ecletica-640	59	43	9	9	NUM
ecletica-640	59	44	)	)	PUNCT
ecletica-640	59	45	,	,	PUNCT
ecletica-640	59	46	we	we	PRON
ecletica-640	59	47	examined	examine	VERB
ecletica-640	59	48	initially	initially	ADV
ecletica-640	59	49	the	the	DET
ecletica-640	59	50	feasybility	feasybility	NOUN
ecletica-640	59	51	of	of	ADP
ecletica-640	59	52	the	the	DET
ecletica-640	59	53	first	first	ADJ
ecletica-640	59	54	strategy	strategy	NOUN
ecletica-640	59	55	using	use	VERB
ecletica-640	59	56	unsubstituted	unsubstituted	ADJ
ecletica-640	59	57	e	e	NOUN
ecletica-640	59	58	-	-	NOUN
ecletica-640	59	59	caprolactone	caprolactone	ADJ
ecletica-640	59	60	(	(	PUNCT
ecletica-640	59	61	10	10	NUM
ecletica-640	59	62	)	)	PUNCT
ecletica-640	59	63	as	as	ADP
ecletica-640	59	64	model	model	NOUN
ecletica-640	59	65	compound	compound	NOUN
ecletica-640	59	66	(	(	PUNCT
ecletica-640	59	67	scheme	scheme	NOUN
ecletica-640	59	68	2	2	NUM
ecletica-640	59	69	)	)	PUNCT
ecletica-640	59	70	.	.	PUNCT
ecletica-640	60	1	all	all	DET
ecletica-640	60	2	attempts	attempt	NOUN
ecletica-640	60	3	of	of	ADP
ecletica-640	60	4	direct	direct	ADJ
ecletica-640	60	5	alkylation	alkylation	NOUN
ecletica-640	60	6	of	of	ADP
ecletica-640	60	7	the	the	DET
ecletica-640	60	8	enolate	enolate	NOUN
ecletica-640	60	9	derived	derive	VERB
ecletica-640	60	10	from	from	ADP
ecletica-640	60	11	(	(	PUNCT
ecletica-640	60	12	10	10	NUM
ecletica-640	60	13	)	)	PUNCT
ecletica-640	60	14	,	,	PUNCT
ecletica-640	60	15	using	use	VERB
ecletica-640	60	16	thf	thf	NOUN
ecletica-640	60	17	,	,	PUNCT
ecletica-640	60	18	hmpa	hmpa	VERB
ecletica-640	60	19	and	and	CCONJ
ecletica-640	60	20	their	their	PRON
ecletica-640	60	21	mixtures	mixture	NOUN
ecletica-640	60	22	at	at	ADP
ecletica-640	60	23	temperatures	temperature	NOUN
ecletica-640	60	24	between	between	ADP
ecletica-640	60	25	-78	-78	PUNCT
ecletica-640	60	26	and	and	CCONJ
ecletica-640	60	27	-30	-30	NUM
ecletica-640	60	28	°	°	PROPN
ecletica-640	60	29	c	c	X
ecletica-640	60	30	,	,	PUNCT
ecletica-640	60	31	produced	produce	VERB
ecletica-640	60	32	only	only	ADV
ecletica-640	60	33	2	2	NUM
ecletica-640	60	34	-	-	PUNCT
ecletica-640	60	35	vinylnaphthalene	vinylnaphthalene	NOUN
ecletica-640	60	36	(	(	PUNCT
ecletica-640	60	37	11	11	NUM
ecletica-640	60	38	)	)	PUNCT
ecletica-640	60	39	.	.	PUNCT
ecletica-640	61	1	at	at	ADP
ecletica-640	61	2	higher	high	ADJ
ecletica-640	61	3	temperature	temperature	NOUN
ecletica-640	61	4	occurred	occur	VERB
ecletica-640	61	5	some	some	DET
ecletica-640	61	6	claisen	claisen	NOUN
ecletica-640	61	7	condensation	condensation	NOUN
ecletica-640	61	8	,	,	PUNCT
ecletica-640	61	9	but	but	CCONJ
ecletica-640	61	10	no	no	DET
ecletica-640	61	11	substitution	substitution	NOUN
ecletica-640	61	12	product	product	NOUN
ecletica-640	61	13	was	be	AUX
ecletica-640	61	14	observed	observe	VERB
ecletica-640	61	15	.	.	PUNCT
ecletica-640	62	1	in	in	ADP
ecletica-640	62	2	order	order	NOUN
ecletica-640	62	3	to	to	PART
ecletica-640	62	4	reduce	reduce	VERB
ecletica-640	62	5	the	the	DET
ecletica-640	62	6	basicity	basicity	NOUN
ecletica-640	62	7	of	of	ADP
ecletica-640	62	8	the	the	DET
ecletica-640	62	9	enolate	enolate	NOUN
ecletica-640	62	10	,	,	PUNCT
ecletica-640	62	11	we	we	PRON
ecletica-640	62	12	prepared	prepare	VERB
ecletica-640	62	13	the	the	DET
ecletica-640	62	14	activated	activate	VERB
ecletica-640	62	15	lactone	lactone	NOUN
ecletica-640	62	16	(	(	PUNCT
ecletica-640	62	17	12	12	NUM
ecletica-640	62	18	)	)	PUNCT
ecletica-640	62	19	.	.	PUNCT
ecletica-640	63	1	its	its	PRON
ecletica-640	63	2	reaction	reaction	NOUN
ecletica-640	63	3	with	with	ADP
ecletica-640	63	4	(	(	PUNCT
ecletica-640	63	5	6	6	NUM
ecletica-640	63	6	)	)	PUNCT
ecletica-640	63	7	(	(	PUNCT
ecletica-640	63	8	x	x	X
ecletica-640	63	9	=	=	NOUN
ecletica-640	63	10	otos	oto	NOUN
ecletica-640	63	11	and	and	CCONJ
ecletica-640	63	12	i	i	PRON
ecletica-640	63	13	)	)	PUNCT
ecletica-640	63	14	–	–	PUNCT
ecletica-640	63	15	even	even	ADV
ecletica-640	63	16	under	under	ADP
ecletica-640	63	17	very	very	ADV
ecletica-640	63	18	smooth	smooth	ADJ
ecletica-640	63	19	conditions	condition	NOUN
ecletica-640	63	20	–	–	PUNCT
ecletica-640	63	21	led	lead	VERB
ecletica-640	63	22	once	once	ADV
ecletica-640	63	23	more	more	ADJ
ecletica-640	63	24	to	to	ADP
ecletica-640	63	25	the	the	DET
ecletica-640	63	26	elimination	elimination	NOUN
ecletica-640	63	27	product	product	NOUN
ecletica-640	63	28	(	(	PUNCT
ecletica-640	63	29	11	11	NUM
ecletica-640	63	30	)	)	PUNCT
ecletica-640	63	31	.	.	PUNCT
ecletica-640	64	1	in	in	ADP
ecletica-640	64	2	the	the	DET
ecletica-640	64	3	hope	hope	NOUN
ecletica-640	64	4	that	that	SCONJ
ecletica-640	64	5	lewis	lewis	PROPN
ecletica-640	64	6	acid	acid	PROPN
ecletica-640	64	7	catalyzed	catalyze	VERB
ecletica-640	64	8	alkylation	alkylation	NOUN
ecletica-640	64	9	could	could	AUX
ecletica-640	64	10	circumvent	circumvent	VERB
ecletica-640	64	11	this	this	DET
ecletica-640	64	12	problem,11	problem,11	NOUN
ecletica-640	64	13	the	the	DET
ecletica-640	64	14	silylated	silylate	VERB
ecletica-640	64	15	derivative	derivative	NOUN
ecletica-640	64	16	(	(	PUNCT
ecletica-640	64	17	13	13	NUM
ecletica-640	64	18	)	)	PUNCT
ecletica-640	64	19	was	be	AUX
ecletica-640	64	20	prepared	prepare	VERB
ecletica-640	64	21	,	,	PUNCT
ecletica-640	64	22	but	but	CCONJ
ecletica-640	64	23	it	it	PRON
ecletica-640	64	24	proved	prove	VERB
ecletica-640	64	25	to	to	PART
ecletica-640	64	26	be	be	AUX
ecletica-640	64	27	unreactive	unreactive	ADJ
ecletica-640	64	28	towards	towards	ADP
ecletica-640	64	29	all	all	DET
ecletica-640	64	30	available	available	ADJ
ecletica-640	64	31	alkylating	alkylating	NOUN
ecletica-640	64	32	reagents	reagent	NOUN
ecletica-640	64	33	(	(	PUNCT
ecletica-640	64	34	6	6	NUM
ecletica-640	64	35	)	)	PUNCT
ecletica-640	64	36	(	(	PUNCT
ecletica-640	64	37	x	x	X
ecletica-640	64	38	=	=	SYM
ecletica-640	64	39	otos	otos	ADJ
ecletica-640	64	40	,	,	PUNCT
ecletica-640	64	41	br	br	NOUN
ecletica-640	64	42	and	and	CCONJ
ecletica-640	64	43	i	i	PRON
ecletica-640	64	44	)	)	PUNCT
ecletica-640	64	45	in	in	ADP
ecletica-640	64	46	the	the	DET
ecletica-640	64	47	presence	presence	NOUN
ecletica-640	64	48	of	of	ADP
ecletica-640	64	49	zinc	zinc	NOUN
ecletica-640	64	50	bromide	bromide	NOUN
ecletica-640	64	51	in	in	ADP
ecletica-640	64	52	dichloromethane	dichloromethane	NOUN
ecletica-640	64	53	at	at	ADP
ecletica-640	64	54	room	room	NOUN
ecletica-640	64	55	temperature	temperature	NOUN
ecletica-640	64	56	.	.	PUNCT
ecletica-640	65	1	the	the	DET
ecletica-640	65	2	more	more	ADV
ecletica-640	65	3	reactive	reactive	ADJ
ecletica-640	65	4	titanium	titanium	NOUN
ecletica-640	65	5	tetrachloride	tetrachloride	NOUN
ecletica-640	65	6	caused	cause	VERB
ecletica-640	65	7	decomposition	decomposition	NOUN
ecletica-640	65	8	of	of	ADP
ecletica-640	65	9	(	(	PUNCT
ecletica-640	65	10	13	13	NUM
ecletica-640	65	11	)	)	PUNCT
ecletica-640	65	12	.	.	PUNCT
ecletica-640	66	1	after	after	ADP
ecletica-640	66	2	the	the	DET
ecletica-640	66	3	failure	failure	NOUN
ecletica-640	66	4	of	of	ADP
ecletica-640	66	5	the	the	DET
ecletica-640	66	6	direct	direct	ADJ
ecletica-640	66	7	alkylation	alkylation	NOUN
ecletica-640	66	8	strategy	strategy	NOUN
ecletica-640	66	9	,	,	PUNCT
ecletica-640	66	10	we	we	PRON
ecletica-640	66	11	examined	examine	VERB
ecletica-640	66	12	the	the	DET
ecletica-640	66	13	stepwise	stepwise	ADJ
ecletica-640	66	14	introduction	introduction	NOUN
ecletica-640	66	15	of	of	ADP
ecletica-640	66	16	the	the	DET
ecletica-640	66	17	2naphthylethyl	2naphthylethyl	PROPN
ecletica-640	66	18	group	group	NOUN
ecletica-640	66	19	(	(	PUNCT
ecletica-640	66	20	scheme	scheme	NOUN
ecletica-640	66	21	3	3	NUM
ecletica-640	66	22	)	)	PUNCT
ecletica-640	66	23	.	.	PUNCT
ecletica-640	67	1	a	a	X
ecletica-640	67	2	-	-	PUNCT
ecletica-640	67	3	methylenation	methylenation	NOUN
ecletica-640	67	4	of	of	ADP
ecletica-640	67	5	(	(	PUNCT
ecletica-640	67	6	10	10	NUM
ecletica-640	67	7	)	)	PUNCT
ecletica-640	67	8	to	to	ADP
ecletica-640	67	9	(	(	PUNCT
ecletica-640	67	10	14	14	NUM
ecletica-640	67	11	)	)	PUNCT
ecletica-640	67	12	followed	follow	VERB
ecletica-640	67	13	by	by	ADP
ecletica-640	67	14	conjugate	conjugate	ADJ
ecletica-640	67	15	addition	addition	NOUN
ecletica-640	67	16	of	of	ADP
ecletica-640	67	17	an	an	DET
ecletica-640	67	18	organomettalic	organomettalic	ADJ
ecletica-640	67	19	reagent	reagent	NOUN
ecletica-640	67	20	seemed	seem	VERB
ecletica-640	67	21	a	a	DET
ecletica-640	67	22	promising	promising	ADJ
ecletica-640	67	23	alternative	alternative	NOUN
ecletica-640	67	24	.	.	PUNCT
ecletica-640	68	1	however	however	ADV
ecletica-640	68	2	,	,	PUNCT
ecletica-640	68	3	literature	literature	NOUN
ecletica-640	68	4	procedures	procedure	NOUN
ecletica-640	68	5	via	via	ADP
ecletica-640	68	6	hydroxymethylation	hydroxymethylation	NOUN
ecletica-640	68	7	4	4	NUM
ecletica-640	68	8	or	or	CCONJ
ecletica-640	68	9	hiomethylation	hiomethylation	NOUN
ecletica-640	68	10	9	9	NUM
ecletica-640	68	11	described	describe	VERB
ecletica-640	68	12	for	for	ADP
ecletica-640	68	13	c	c	PROPN
ecletica-640	68	14	and	and	CCONJ
ecletica-640	68	15	d	d	PROPN
ecletica-640	68	16	-	-	PUNCT
ecletica-640	68	17	lactones	lactone	NOUN
ecletica-640	68	18	produced	produce	VERB
ecletica-640	68	19	only	only	ADJ
ecletica-640	68	20	decomposition	decomposition	NOUN
ecletica-640	68	21	of	of	ADP
ecletica-640	68	22	the	the	DET
ecletica-640	68	23	e	e	NOUN
ecletica-640	68	24	-	-	NOUN
ecletica-640	68	25	lactone	lactone	NOUN
ecletica-640	68	26	.	.	PUNCT
ecletica-640	69	1	another	another	DET
ecletica-640	69	2	possibility	possibility	NOUN
ecletica-640	69	3	was	be	AUX
ecletica-640	69	4	the	the	DET
ecletica-640	69	5	preparation	preparation	NOUN
ecletica-640	69	6	of	of	ADP
ecletica-640	69	7	the	the	DET
ecletica-640	69	8	aldehyde	aldehyde	NOUN
ecletica-640	69	9	-	-	PUNCT
ecletica-640	69	10	lactone	lactone	NOUN
ecletica-640	69	11	(	(	PUNCT
ecletica-640	69	12	16	16	NUM
ecletica-640	69	13	)	)	PUNCT
ecletica-640	69	14	.	.	PUNCT
ecletica-640	70	1	subsequent	subsequent	ADJ
ecletica-640	70	2	grignard	grignard	ADJ
ecletica-640	70	3	reaction	reaction	NOUN
ecletica-640	70	4	should	should	AUX
ecletica-640	70	5	then	then	ADV
ecletica-640	70	6	introduce	introduce	VERB
ecletica-640	70	7	the	the	DET
ecletica-640	70	8	2	2	NUM
ecletica-640	70	9	-	-	PUNCT
ecletica-640	70	10	naphthyl	naphthyl	NOUN
ecletica-640	70	11	moiety	moiety	NOUN
ecletica-640	70	12	and	and	CCONJ
ecletica-640	70	13	catalytic	catalytic	ADJ
ecletica-640	70	14	hydrogenation	hydrogenation	NOUN
ecletica-640	70	15	would	would	AUX
ecletica-640	70	16	lead	lead	VERB
ecletica-640	70	17	to	to	ADP
ecletica-640	70	18	an	an	DET
ecletica-640	70	19	intermediate	intermediate	NOUN
ecletica-640	70	20	of	of	ADP
ecletica-640	70	21	type	type	NOUN
ecletica-640	70	22	(	(	PUNCT
ecletica-640	70	23	4	4	NUM
ecletica-640	70	24	)	)	PUNCT
ecletica-640	70	25	.	.	PUNCT
ecletica-640	71	1	indeed	indeed	ADV
ecletica-640	71	2	,	,	PUNCT
ecletica-640	71	3	(	(	PUNCT
ecletica-640	71	4	10	10	NUM
ecletica-640	71	5	)	)	PUNCT
ecletica-640	71	6	was	be	AUX
ecletica-640	71	7	successfully	successfully	ADV
ecletica-640	71	8	allylated	allylate	VERB
ecletica-640	71	9	to	to	ADP
ecletica-640	71	10	(	(	PUNCT
ecletica-640	71	11	15	15	NUM
ecletica-640	71	12	)	)	PUNCT
ecletica-640	71	13	and	and	CCONJ
ecletica-640	71	14	then	then	ADV
ecletica-640	71	15	cleaved	cleaved	ADJ
ecletica-640	71	16	to	to	ADP
ecletica-640	71	17	(	(	PUNCT
ecletica-640	71	18	16	16	NUM
ecletica-640	71	19	)	)	PUNCT
ecletica-640	71	20	,	,	PUNCT
ecletica-640	71	21	as	as	SCONJ
ecletica-640	71	22	evidenced	evidence	VERB
ecletica-640	71	23	by	by	ADP
ecletica-640	71	24	spectroscopic	spectroscopic	ADJ
ecletica-640	71	25	means	mean	NOUN
ecletica-640	71	26	,	,	PUNCT
ecletica-640	71	27	but	but	CCONJ
ecletica-640	71	28	the	the	DET
ecletica-640	71	29	latter	latter	ADJ
ecletica-640	71	30	decomposed	decompose	VERB
ecletica-640	71	31	during	during	ADP
ecletica-640	71	32	the	the	DET
ecletica-640	71	33	work	work	NOUN
ecletica-640	71	34	up	up	ADP
ecletica-640	71	35	procedure	procedure	NOUN
ecletica-640	71	36	.	.	PUNCT
ecletica-640	72	1	summarizing	summarize	VERB
ecletica-640	72	2	the	the	DET
ecletica-640	72	3	different	different	ADJ
ecletica-640	72	4	variants	variant	NOUN
ecletica-640	72	5	of	of	ADP
ecletica-640	72	6	the	the	DET
ecletica-640	72	7	alkylation	alkylation	NOUN
ecletica-640	72	8	strategy	strategy	NOUN
ecletica-640	72	9	,	,	PUNCT
ecletica-640	72	10	we	we	PRON
ecletica-640	72	11	can	can	AUX
ecletica-640	72	12	conclude	conclude	VERB
ecletica-640	72	13	that	that	SCONJ
ecletica-640	72	14	a	a	DET
ecletica-640	72	15	cationic	cationic	ADJ
ecletica-640	72	16	2	2	NUM
ecletica-640	72	17	-	-	PUNCT
ecletica-640	72	18	naphthylethyl	naphthylethyl	ADV
ecletica-640	72	19	synthon	synthon	ADJ
ecletica-640	72	20	is	be	AUX
ecletica-640	72	21	not	not	PART
ecletica-640	72	22	suitable	suitable	ADJ
ecletica-640	72	23	for	for	ADP
ecletica-640	72	24	substitution	substitution	NOUN
ecletica-640	72	25	reactions	reaction	NOUN
ecletica-640	72	26	in	in	ADP
ecletica-640	72	27	basic	basic	ADJ
ecletica-640	72	28	as	as	ADV
ecletica-640	72	29	well	well	ADV
ecletica-640	72	30	in	in	ADP
ecletica-640	72	31	lewis	lewis	PROPN
ecletica-640	72	32	acid	acid	PROPN
ecletica-640	72	33	catalyzed	catalyze	VERB
ecletica-640	72	34	conditions	condition	NOUN
ecletica-640	72	35	.	.	PUNCT
ecletica-640	73	1	furthermore	furthermore	ADV
ecletica-640	73	2	,	,	PUNCT
ecletica-640	73	3	e	e	NOUN
ecletica-640	73	4	-	-	NOUN
ecletica-640	73	5	lactones	lactone	NOUN
ecletica-640	73	6	proved	prove	VERB
ecletica-640	73	7	to	to	PART
ecletica-640	73	8	be	be	AUX
ecletica-640	73	9	unstable	unstable	ADJ
ecletica-640	73	10	when	when	SCONJ
ecletica-640	73	11	stepwise	stepwise	ADJ
ecletica-640	73	12	introduction	introduction	NOUN
ecletica-640	73	13	of	of	ADP
ecletica-640	73	14	the	the	DET
ecletica-640	73	15	substituted	substitute	VERB
ecletica-640	73	16	was	be	AUX
ecletica-640	73	17	tried	try	VERB
ecletica-640	73	18	.	.	PUNCT
ecletica-640	74	1	in	in	ADP
ecletica-640	74	2	consequence	consequence	NOUN
ecletica-640	74	3	,	,	PUNCT
ecletica-640	74	4	our	our	PRON
ecletica-640	74	5	attention	attention	NOUN
ecletica-640	74	6	moved	move	VERB
ecletica-640	74	7	to	to	ADP
ecletica-640	74	8	the	the	DET
ecletica-640	74	9	second	second	ADJ
ecletica-640	74	10	main	main	ADJ
ecletica-640	74	11	strategy	strategy	NOUN
ecletica-640	74	12	of	of	ADP
ecletica-640	74	13	scheme	scheme	NOUN
ecletica-640	74	14	1	1	NUM
ecletica-640	74	15	.	.	PUNCT
ecletica-640	75	1	because	because	SCONJ
ecletica-640	75	2	of	of	ADP
ecletica-640	75	3	the	the	DET
ecletica-640	75	4	unattractive	unattractive	ADJ
ecletica-640	75	5	preparation	preparation	NOUN
ecletica-640	75	6	of	of	ADP
ecletica-640	75	7	the	the	DET
ecletica-640	75	8	unsaturated	unsaturated	ADJ
ecletica-640	75	9	alcohol	alcohol	NOUN
ecletica-640	75	10	(	(	PUNCT
ecletica-640	75	11	9	9	NUM
ecletica-640	75	12	)	)	PUNCT
ecletica-640	75	13	described	describe	VERB
ecletica-640	75	14	in	in	ADP
ecletica-640	75	15	the	the	DET
ecletica-640	75	16	literature,13	literature,13	NOUN
ecletica-640	75	17	once	once	ADV
ecletica-640	75	18	more	more	ADV
ecletica-640	75	19	a	a	DET
ecletica-640	75	20	model	model	NOUN
ecletica-640	75	21	compound	compound	NOUN
ecletica-640	75	22	was	be	AUX
ecletica-640	75	23	used	use	VERB
ecletica-640	75	24	for	for	ADP
ecletica-640	75	25	explorative	explorative	ADJ
ecletica-640	75	26	work	work	NOUN
ecletica-640	75	27	.	.	PUNCT
ecletica-640	76	1	racemic	racemic	ADJ
ecletica-640	76	2	citronellol	citronellol	NOUN
ecletica-640	76	3	,	,	PUNCT
ecletica-640	76	4	which	which	PRON
ecletica-640	76	5	differs	differ	VERB
ecletica-640	76	6	from	from	ADP
ecletica-640	76	7	(	(	PUNCT
ecletica-640	76	8	9	9	NUM
ecletica-640	76	9	)	)	PUNCT
ecletica-640	76	10	by	by	ADP
ecletica-640	76	11	one	one	NUM
ecletica-640	76	12	carbon	carbon	NOUN
ecletica-640	76	13	atom	atom	NOUN
ecletica-640	76	14	more	more	ADV
ecletica-640	76	15	in	in	ADP
ecletica-640	76	16	the	the	DET
ecletica-640	76	17	chain	chain	NOUN
ecletica-640	76	18	and	and	CCONJ
ecletica-640	76	19	by	by	ADP
ecletica-640	76	20	the	the	DET
ecletica-640	76	21	position	position	NOUN
ecletica-640	76	22	of	of	ADP
ecletica-640	76	23	the	the	DET
ecletica-640	76	24	methyl	methyl	NOUN
ecletica-640	76	25	group	group	NOUN
ecletica-640	76	26	,	,	PUNCT
ecletica-640	76	27	was	be	AUX
ecletica-640	76	28	transformed	transform	VERB
ecletica-640	76	29	to	to	ADP
ecletica-640	76	30	the	the	DET
ecletica-640	76	31	known	know	VERB
ecletica-640	76	32	epoxide	epoxide	NOUN
ecletica-640	76	33	(	(	PUNCT
ecletica-640	76	34	17	17	NUM
ecletica-640	76	35	)	)	PUNCT
ecletica-640	77	1	.6	.6	NUM
ecletica-640	77	2	reaction	reaction	NOUN
ecletica-640	77	3	with	with	ADP
ecletica-640	77	4	an	an	DET
ecletica-640	77	5	excess	excess	NOUN
ecletica-640	77	6	of	of	ADP
ecletica-640	77	7	the	the	DET
ecletica-640	77	8	cuprate	cuprate	NOUN
ecletica-640	77	9	(	(	PUNCT
ecletica-640	77	10	8)	8)	NUM
ecletica-640	77	11	,	,	PUNCT
ecletica-640	77	12	prepared	prepare	VERB
ecletica-640	77	13	from	from	ADP
ecletica-640	77	14	(	(	PUNCT
ecletica-640	77	15	7	7	NUM
ecletica-640	77	16	)	)	PUNCT
ecletica-640	77	17	(	(	PUNCT
ecletica-640	77	18	x	x	X
ecletica-640	77	19	=	=	VERB
ecletica-640	77	20	i	i	PROPN
ecletica-640	77	21	)	)	PUNCT
ecletica-640	77	22	,	,	PUNCT
ecletica-640	77	23	produced	produce	VERB
ecletica-640	77	24	the	the	DET
ecletica-640	77	25	crystalline	crystalline	ADJ
ecletica-640	77	26	diol	diol	NOUN
ecletica-640	77	27	(	(	PUNCT
ecletica-640	77	28	18	18	NUM
ecletica-640	77	29	)	)	PUNCT
ecletica-640	77	30	,	,	PUNCT
ecletica-640	77	31	probably	probably	ADV
ecletica-640	77	32	as	as	ADP
ecletica-640	77	33	a	a	DET
ecletica-640	77	34	mixture	mixture	NOUN
ecletica-640	77	35	of	of	ADP
ecletica-640	77	36	diastereomers	diastereomer	NOUN
ecletica-640	77	37	(	(	PUNCT
ecletica-640	77	38	scheme	scheme	NOUN
ecletica-640	77	39	4	4	NUM
ecletica-640	77	40	)	)	PUNCT
ecletica-640	77	41	.	.	PUNCT
ecletica-640	78	1	the	the	DET
ecletica-640	78	2	only	only	ADJ
ecletica-640	78	3	side	side	NOUN
ecletica-640	78	4	product	product	NOUN
ecletica-640	78	5	was	be	AUX
ecletica-640	78	6	1,4	1,4	NUM
ecletica-640	78	7	-	-	PUNCT
ecletica-640	78	8	di-2	di-2	NOUN
ecletica-640	78	9	-	-	PUNCT
ecletica-640	78	10	naphthylbutane	naphthylbutane	NOUN
ecletica-640	78	11	5	5	NUM
ecletica-640	78	12	formed	form	VERB
ecletica-640	78	13	by	by	ADP
ecletica-640	78	14	thermal	thermal	ADJ
ecletica-640	78	15	dimerization	dimerization	NOUN
ecletica-640	78	16	of	of	ADP
ecletica-640	78	17	the	the	DET
ecletica-640	78	18	cuprate	cuprate	NOUN
ecletica-640	78	19	(	(	PUNCT
ecletica-640	78	20	8)	8)	NUM
ecletica-640	78	21	.	.	PUNCT
ecletica-640	78	22	conclusion	conclusion	NOUN
ecletica-640	78	23	the	the	DET
ecletica-640	78	24	successful	successful	ADJ
ecletica-640	78	25	coupling	coupling	NOUN
ecletica-640	78	26	reaction	reaction	NOUN
ecletica-640	78	27	(	(	PUNCT
ecletica-640	78	28	scheme	scheme	NOUN
ecletica-640	78	29	4	4	NUM
ecletica-640	78	30	)	)	PUNCT
ecletica-640	78	31	demonstrates	demonstrate	VERB
ecletica-640	78	32	that	that	SCONJ
ecletica-640	78	33	the	the	DET
ecletica-640	78	34	carbanionic	carbanionic	ADJ
ecletica-640	78	35	2	2	NUM
ecletica-640	78	36	-	-	PUNCT
ecletica-640	78	37	naphthylethyl	naphthylethyl	ADV
ecletica-640	78	38	synthon	synthon	ADJ
ecletica-640	78	39	is	be	AUX
ecletica-640	78	40	more	more	ADV
ecletica-640	78	41	suitable	suitable	ADJ
ecletica-640	78	42	for	for	ADP
ecletica-640	78	43	c	c	NOUN
ecletica-640	78	44	-	-	PUNCT
ecletica-640	78	45	c	c	NOUN
ecletica-640	78	46	bond	bond	NOUN
ecletica-640	78	47	formation	formation	NOUN
ecletica-640	78	48	than	than	ADP
ecletica-640	78	49	the	the	DET
ecletica-640	78	50	cationic	cationic	ADJ
ecletica-640	78	51	one	one	NUM
ecletica-640	78	52	.	.	PUNCT
ecletica-640	79	1	it	it	PRON
ecletica-640	79	2	opens	open	VERB
ecletica-640	79	3	now	now	ADV
ecletica-640	79	4	the	the	DET
ecletica-640	79	5	possibility	possibility	NOUN
ecletica-640	79	6	to	to	PART
ecletica-640	79	7	obtain	obtain	VERB
ecletica-640	79	8	the	the	DET
ecletica-640	79	9	key	key	ADJ
ecletica-640	79	10	-	-	PUNCT
ecletica-640	79	11	intermediate	intermediate	ADJ
ecletica-640	79	12	(	(	PUNCT
ecletica-640	79	13	3	3	NUM
ecletica-640	79	14	)	)	PUNCT
ecletica-640	79	15	by	by	ADP
ecletica-640	79	16	an	an	DET
ecletica-640	79	17	analogous	analogous	ADJ
ecletica-640	79	18	reaction	reaction	NOUN
ecletica-640	79	19	.	.	PUNCT
ecletica-640	80	1	the	the	DET
ecletica-640	80	2	development	development	NOUN
ecletica-640	80	3	of	of	ADP
ecletica-640	80	4	a	a	DET
ecletica-640	80	5	practical	practical	ADJ
ecletica-640	80	6	synthesis	synthesis	NOUN
ecletica-640	80	7	of	of	ADP
ecletica-640	80	8	the	the	DET
ecletica-640	80	9	unsaturated	unsaturated	ADJ
ecletica-640	80	10	alcohol	alcohol	NOUN
ecletica-640	80	11	(	(	PUNCT
ecletica-640	80	12	9	9	NUM
ecletica-640	80	13	)	)	PUNCT
ecletica-640	80	14	as	as	ADP
ecletica-640	80	15	a	a	DET
ecletica-640	80	16	pure	pure	ADJ
ecletica-640	80	17	enantiomer	enantiomer	NOUN
ecletica-640	80	18	and	and	CCONJ
ecletica-640	80	19	its	its	PRON
ecletica-640	80	20	use	use	NOUN
ecletica-640	80	21	in	in	ADP
ecletica-640	80	22	the	the	DET
ecletica-640	80	23	asymmetric	asymmetric	ADJ
ecletica-640	80	24	synthesis	synthesis	NOUN
ecletica-640	80	25	of	of	ADP
ecletica-640	80	26	cordiaquinone	cordiaquinone	PROPN
ecletica-640	80	27	a	a	PRON
ecletica-640	80	28	is	be	AUX
ecletica-640	80	29	now	now	ADV
ecletica-640	80	30	in	in	ADP
ecletica-640	80	31	progress	progress	NOUN
ecletica-640	80	32	.	.	PUNCT
ecletica-640	81	1	acknowledgements	acknowledgement	NOUN
ecletica-640	81	2	the	the	DET
ecletica-640	81	3	authors	author	NOUN
ecletica-640	81	4	thank	thank	VERB
ecletica-640	81	5	for	for	ADP
ecletica-640	81	6	fellowships	fellowship	NOUN
ecletica-640	81	7	from	from	ADP
ecletica-640	81	8	cnpq	cnpq	NOUN
ecletica-640	81	9	and	and	CCONJ
ecletica-640	81	10	financial	financial	ADJ
ecletica-640	81	11	support	support	NOUN
ecletica-640	81	12	from	from	ADP
ecletica-640	81	13	facepe	facepe	NOUN
ecletica-640	81	14	.	.	PUNCT
ecletica-640	82	1	batalini	batalini	PROPN
ecletica-640	82	2	,	,	PUNCT
ecletica-640	82	3	c.	c.	PROPN
ecletica-640	82	4	,	,	PUNCT
ecletica-640	82	5	bieber	bieber	PROPN
ecletica-640	82	6	,	,	PUNCT
ecletica-640	82	7	l.w	l.w	PROPN
ecletica-640	82	8	.	.	PROPN
ecletica-640	82	9	estudos	estudos	PROPN
ecletica-640	82	10	modelo	modelo	PROPN
ecletica-640	82	11	da	da	PROPN
ecletica-640	82	12	síntese	síntese	PROPN
ecletica-640	82	13	do	do	VERB
ecletica-640	82	14	meroterpenóide	meroterpenóide	PROPN
ecletica-640	82	15	natural	natural	ADJ
ecletica-640	82	16	cordiaquinona	cordiaquinona	PROPN
ecletica-640	82	17	a.	a.	PROPN
ecletica-640	82	18	ecl	ecl	PROPN
ecletica-640	82	19	.	.	PROPN
ecletica-640	82	20	quím	quím	PROPN
ecletica-640	82	21	.	.	PUNCT
ecletica-640	83	1	(	(	PUNCT
ecletica-640	83	2	são	são	PROPN
ecletica-640	83	3	paulo	paulo	PROPN
ecletica-640	83	4	)	)	PUNCT
ecletica-640	83	5	,	,	PUNCT
ecletica-640	83	6	v.26	v.26	X
ecletica-640	83	7	,	,	PUNCT
ecletica-640	83	8	p.	p.	NOUN
ecletica-640	83	9	,	,	PUNCT
ecletica-640	83	10	2001	2001	NUM
ecletica-640	83	11	.	.	PUNCT
ecletica-640	84	1	resumo	resumo	ADJ
ecletica-640	84	2	:	:	PUNCT
ecletica-640	84	3	duas	duas	PROPN
ecletica-640	84	4	estratégias	estratégia	VERB
ecletica-640	84	5	principais	principais	PROPN
ecletica-640	84	6	visando	visando	PROPN
ecletica-640	84	7	a	a	DET
ecletica-640	84	8	síntese	síntese	NOUN
ecletica-640	84	9	do	do	AUX
ecletica-640	84	10	meroterpenóide	meroterpenóide	VERB
ecletica-640	84	11	natural	natural	ADJ
ecletica-640	84	12	cordiaquinona	cordiaquinona	NOUN
ecletica-640	84	13	a	a	DET
ecletica-640	84	14	(	(	PUNCT
ecletica-640	84	15	1	1	NUM
ecletica-640	84	16	)	)	PUNCT
ecletica-640	84	17	–	–	PUNCT
ecletica-640	84	18	isolada	isolada	PROPN
ecletica-640	84	19	das	das	PROPN
ecletica-640	84	20	raízes	raíze	VERB
ecletica-640	85	1	de	de	PROPN
ecletica-640	85	2	cordia	cordia	PROPN
ecletica-640	85	3	corymbosa	corymbosa	PROPN
ecletica-640	85	4	g.	g.	PROPN
ecletica-640	85	5	don	don	PROPN
ecletica-640	85	6	(	(	PUNCT
ecletica-640	85	7	boraginaceae	boraginaceae	PROPN
ecletica-640	85	8	)	)	PUNCT
ecletica-640	85	9	–	–	PUNCT
ecletica-640	85	10	foram	foram	NOUN
ecletica-640	85	11	testadas	testada	NOUN
ecletica-640	85	12	em	em	PRON
ecletica-640	85	13	compostos	composto	VERB
ecletica-640	85	14	modelo	modelo	NOUN
ecletica-640	85	15	.	.	PUNCT
ecletica-640	86	1	enquanto	enquanto	ADP
ecletica-640	86	2	todas	todas	PROPN
ecletica-640	86	3	as	as	SCONJ
ecletica-640	86	4	variantes	variantes	PROPN
ecletica-640	86	5	envolvendo	envolvendo	VERB
ecletica-640	86	6	a	a	DET
ecletica-640	86	7	alquilação	alquilação	NOUN
ecletica-640	86	8	de	de	X
ecletica-640	86	9	e	e	PROPN
ecletica-640	86	10	-	-	NOUN
ecletica-640	86	11	caprolactona	caprolactona	ADJ
ecletica-640	86	12	(	(	PUNCT
ecletica-640	86	13	10	10	NUM
ecletica-640	86	14	)	)	PUNCT
ecletica-640	86	15	falharam	falharam	NOUN
ecletica-640	86	16	,	,	PUNCT
ecletica-640	86	17	o	o	NOUN
ecletica-640	86	18	acoplamento	acoplamento	ADP
ecletica-640	86	19	de	de	X
ecletica-640	86	20	epoxicitronelol	epoxicitronelol	X
ecletica-640	86	21	(	(	PUNCT
ecletica-640	86	22	17	17	NUM
ecletica-640	86	23	)	)	PUNCT
ecletica-640	86	24	com	com	NOUN
ecletica-640	86	25	um	um	INTJ
ecletica-640	86	26	organocuprato	organocuprato	PROPN
ecletica-640	86	27	apropriado	apropriado	NOUN
ecletica-640	86	28	ocorreu	ocorreu	NOUN
ecletica-640	86	29	no	no	DET
ecletica-640	86	30	sentido	sentido	NOUN
ecletica-640	86	31	esperado	esperado	X
ecletica-640	86	32	.	.	PUNCT
ecletica-640	87	1	palavras	palavra	NOUN
ecletica-640	87	2	-	-	PUNCT
ecletica-640	87	3	chave	chave	NOUN
ecletica-640	87	4	:	:	PUNCT
ecletica-640	87	5	naftoquinona	naftoquinona	NOUN
ecletica-640	87	6	meroterpenóide	meroterpenóide	NOUN
ecletica-640	87	7	,	,	PUNCT
ecletica-640	87	8	cordia	cordia	PROPN
ecletica-640	87	9	corymbosa	corymbosa	PROPN
ecletica-640	87	10	,	,	PUNCT
ecletica-640	87	11	boraginaceae	boraginaceae	PROPN
ecletica-640	87	12	ecaprolactona	ecaprolactona	PROPN
ecletica-640	87	13	,	,	PUNCT
ecletica-640	87	14	epoxicitronelol	epoxicitronelol	NOUN
ecletica-640	87	15	,	,	PUNCT
ecletica-640	87	16	organocuprato	organocuprato	PROPN
ecletica-640	87	17	.	.	PUNCT
ecletica-640	88	1	references	reference	NOUN
ecletica-640	88	2	1	1	NUM
ecletica-640	88	3	bentley	bentley	PROPN
ecletica-640	88	4	,	,	PUNCT
ecletica-640	88	5	m.d	m.d	PROPN
ecletica-640	88	6	.	.	PROPN
ecletica-640	88	7	;	;	PUNCT
ecletica-640	88	8	dewar	dewar	PROPN
ecletica-640	88	9	,	,	PUNCT
ecletica-640	88	10	m.j.s	m.j.s	PROPN
ecletica-640	88	11	.	.	PUNCT
ecletica-640	89	1	the	the	DET
ecletica-640	89	2	solvolysis	solvolysis	NOUN
ecletica-640	89	3	of	of	ADP
ecletica-640	89	4	2	2	NUM
ecletica-640	89	5	-	-	PUNCT
ecletica-640	89	6	arylethyl	arylethyl	NOUN
ecletica-640	89	7	-	-	PUNCT
ecletica-640	89	8	p	p	NOUN
ecletica-640	89	9	-	-	PUNCT
ecletica-640	89	10	toluenesulfonates	toluenesulfonate	NOUN
ecletica-640	89	11	.	.	PUNCT
ecletica-640	90	1	j.	j.	PROPN
ecletica-640	90	2	am	am	PROPN
ecletica-640	90	3	.	.	PUNCT
ecletica-640	91	1	chem	chem	NOUN
ecletica-640	91	2	.	.	PUNCT
ecletica-640	92	1	soc	soc	PROPN
ecletica-640	92	2	.	.	PUNCT
ecletica-640	92	3	,	,	PUNCT
ecletica-640	92	4	v.92	v.92	PROPN
ecletica-640	92	5	,	,	PUNCT
ecletica-640	92	6	p.3996	p.3996	NOUN
ecletica-640	92	7	-	-	SYM
ecletica-640	92	8	4002	4002	NUM
ecletica-640	92	9	,	,	PUNCT
ecletica-640	92	10	1970	1970	NUM
ecletica-640	92	11	.	.	PUNCT
ecletica-640	93	1	[	[	PUNCT
ecletica-640	93	2	links	link	NOUN
ecletica-640	93	3	]	]	PUNCT
ecletica-640	93	4	2	2	NUM
ecletica-640	93	5	bieber	bieber	NOUN
ecletica-640	93	6	,	,	PUNCT
ecletica-640	93	7	l.w	l.w	PROPN
ecletica-640	93	8	.	.	PROPN
ecletica-640	93	9	et	et	PROPN
ecletica-640	93	10	al	al	PROPN
ecletica-640	93	11	.	.	PROPN
ecletica-640	94	1	meroterpenoid	meroterpenoid	PROPN
ecletica-640	94	2	naphthoquinones	naphthoquinone	VERB
ecletica-640	94	3	from	from	ADP
ecletica-640	94	4	cordia	cordia	PROPN
ecletica-640	94	5	corymbosa	corymbosa	PROPN
ecletica-640	94	6	.	.	PUNCT
ecletica-640	95	1	phytochemistry	phytochemistry	NOUN
ecletica-640	95	2	,	,	PUNCT
ecletica-640	95	3	v.29	v.29	PROPN
ecletica-640	95	4	,	,	PUNCT
ecletica-640	95	5	n.6	n.6	PUNCT
ecletica-640	95	6	,	,	PUNCT
ecletica-640	95	7	p.1955	p.1955	NOUN
ecletica-640	95	8	-	-	NUM
ecletica-640	95	9	1959	1959	NUM
ecletica-640	95	10	,	,	PUNCT
ecletica-640	95	11	1990	1990	NUM
ecletica-640	95	12	.	.	PUNCT
ecletica-640	96	1	[	[	PUNCT
ecletica-640	96	2	links	link	NOUN
ecletica-640	96	3	]	]	PUNCT
ecletica-640	96	4	3	3	NUM
ecletica-640	96	5	bieber	bieber	NOUN
ecletica-640	96	6	,	,	PUNCT
ecletica-640	96	7	l.w	l.w	PROPN
ecletica-640	96	8	.	.	PROPN
ecletica-640	96	9	et	et	PROPN
ecletica-640	97	1	al	al	PROPN
ecletica-640	97	2	.	.	PUNCT
ecletica-640	97	3	further	further	PROPN
ecletica-640	97	4	meroterpenoid	meroterpenoid	PROPN
ecletica-640	97	5	naphthoquinones	naphthoquinone	NOUN
ecletica-640	97	6	from	from	ADP
ecletica-640	97	7	cordia	cordia	PROPN
ecletica-640	97	8	corymbosa	corymbosa	PROPN
ecletica-640	97	9	.	.	PUNCT
ecletica-640	98	1	phytochemistry	phytochemistry	NOUN
ecletica-640	98	2	,	,	PUNCT
ecletica-640	98	3	v.35	v.35	NOUN
ecletica-640	98	4	,	,	PUNCT
ecletica-640	98	5	p.1027	p.1027	NOUN
ecletica-640	98	6	-	-	PUNCT
ecletica-640	98	7	1028	1028	NUM
ecletica-640	98	8	,	,	PUNCT
ecletica-640	98	9	1994	1994	NUM
ecletica-640	98	10	.	.	PUNCT
ecletica-640	99	1	[	[	PUNCT
ecletica-640	99	2	links	link	NOUN
ecletica-640	99	3	]	]	PUNCT
ecletica-640	99	4	javascript	javascript	NOUN
ecletica-640	99	5	:	:	PUNCT
ecletica-640	99	6	void(0	void(0	PROPN
ecletica-640	99	7	)	)	PUNCT
ecletica-640	99	8	;	;	PUNCT
ecletica-640	99	9	javascript	javascript	NOUN
ecletica-640	99	10	:	:	PUNCT
ecletica-640	99	11	void(0	void(0	PROPN
ecletica-640	99	12	)	)	PUNCT
ecletica-640	99	13	;	;	PUNCT
ecletica-640	99	14	javascript	javascript	NOUN
ecletica-640	99	15	:	:	PUNCT
ecletica-640	99	16	void(0	void(0	PROPN
ecletica-640	99	17	)	)	PUNCT
ecletica-640	99	18	;	;	PUNCT
ecletica-640	99	19	4	4	NUM
ecletica-640	99	20	grieco	grieco	PROPN
ecletica-640	99	21	,	,	PUNCT
ecletica-640	99	22	p.a	p.a	PROPN
ecletica-640	99	23	.	.	PROPN
ecletica-640	99	24	;	;	PUNCT
ecletica-640	99	25	hiroi	hiroi	PROPN
ecletica-640	99	26	,	,	PUNCT
ecletica-640	99	27	k.	k.	PROPN
ecletica-640	99	28	model	model	PROPN
ecletica-640	99	29	studies	study	NOUN
ecletica-640	99	30	directed	direct	VERB
ecletica-640	99	31	toward	toward	ADP
ecletica-640	99	32	the	the	DET
ecletica-640	99	33	total	total	ADJ
ecletica-640	99	34	synthesis	synthesis	NOUN
ecletica-640	99	35	of	of	ADP
ecletica-640	99	36	vernolepin	vernolepin	NOUN
ecletica-640	99	37	:	:	PUNCT
ecletica-640	99	38	construction	construction	NOUN
ecletica-640	99	39	of	of	ADP
ecletica-640	99	40	the	the	DET
ecletica-640	99	41	a	a	DET
ecletica-640	99	42	-	-	PUNCT
ecletica-640	99	43	methylene	methylene	NOUN
ecletica-640	99	44	-	-	PUNCT
ecletica-640	99	45	d	d	NOUN
ecletica-640	99	46	-	-	PUNCT
ecletica-640	99	47	lactone	lactone	ADJ
ecletica-640	99	48	portion	portion	NOUN
ecletica-640	99	49	of	of	ADP
ecletica-640	99	50	vernolepin	vernolepin	NOUN
ecletica-640	99	51	.	.	PUNCT
ecletica-640	100	1	tetrahedron	tetrahedron	NOUN
ecletica-640	100	2	letters	letter	NOUN
ecletica-640	100	3	,	,	PUNCT
ecletica-640	100	4	n.21	n.21	PROPN
ecletica-640	100	5	,	,	PUNCT
ecletica-640	100	6	p.1831	p.1831	PROPN
ecletica-640	100	7	-	-	PUNCT
ecletica-640	100	8	1834	1834	NUM
ecletica-640	100	9	,	,	PUNCT
ecletica-640	100	10	1973	1973	NUM
ecletica-640	100	11	.	.	PUNCT
ecletica-640	101	1	[	[	PUNCT
ecletica-640	101	2	links	link	NOUN
ecletica-640	101	3	]	]	PUNCT
ecletica-640	101	4	5	5	NUM
ecletica-640	101	5	karrer	karrer	NOUN
ecletica-640	101	6	,	,	PUNCT
ecletica-640	101	7	p.	p.	NOUN
ecletica-640	101	8	et	et	NOUN
ecletica-640	102	1	al	al	PROPN
ecletica-640	102	2	.	.	PUNCT
ecletica-640	103	1	synthese	synthese	PROPN
ecletica-640	103	2	des	des	PROPN
ecletica-640	103	3	2	2	NUM
ecletica-640	103	4	-	-	PUNCT
ecletica-640	103	5	phytyl	phytyl	NOUN
ecletica-640	103	6	-	-	PUNCT
ecletica-640	103	7	naphtochinons-1,4	naphtochinons-1,4	NOUN
ecletica-640	103	8	.	.	PUNCT
ecletica-640	104	1	helv	helv	PROPN
ecletica-640	104	2	.	.	PUNCT
ecletica-640	105	1	chim	chim	PROPN
ecletica-640	105	2	.	.	PUNCT
ecletica-640	106	1	acta	acta	PROPN
ecletica-640	106	2	,	,	PUNCT
ecletica-640	106	3	v.23	v.23	PROPN
ecletica-640	106	4	,	,	PUNCT
ecletica-640	106	5	p.585	p.585	ADV
ecletica-640	106	6	-	-	PUNCT
ecletica-640	106	7	590	590	NUM
ecletica-640	106	8	,	,	PUNCT
ecletica-640	106	9	1940	1940	NUM
ecletica-640	106	10	.	.	PUNCT
ecletica-640	107	1	[	[	PUNCT
ecletica-640	107	2	links	link	NOUN
ecletica-640	107	3	]	]	PUNCT
ecletica-640	107	4	6	6	NUM
ecletica-640	107	5	koetz	koetz	PROPN
ecletica-640	107	6	,	,	PUNCT
ecletica-640	107	7	a.	a.	NOUN
ecletica-640	107	8	;	;	PUNCT
ecletica-640	107	9	steche	steche	NOUN
ecletica-640	107	10	,	,	PUNCT
ecletica-640	107	11	t.	t.	PROPN
ecletica-640	107	12	über	über	PROPN
ecletica-640	107	13	die	die	VERB
ecletica-640	107	14	stufenweise	stufenweise	PROPN
ecletica-640	107	15	oxydation	oxydation	NOUN
ecletica-640	107	16	des	des	PROPN
ecletica-640	107	17	citronellols	citronellols	PROPN
ecletica-640	107	18	und	und	VERB
ecletica-640	107	19	geraniols	geraniol	NOUN
ecletica-640	107	20	.	.	PUNCT
ecletica-640	108	1	j.	j.	PROPN
ecletica-640	108	2	prakt	prakt	PROPN
ecletica-640	108	3	.	.	PUNCT
ecletica-640	109	1	chem	chem	PROPN
ecletica-640	109	2	.	.	PUNCT
ecletica-640	109	3	,	,	PUNCT
ecletica-640	109	4	v.107	v.107	NUM
ecletica-640	109	5	,	,	PUNCT
ecletica-640	109	6	p.193	p.193	NOUN
ecletica-640	109	7	-	-	NOUN
ecletica-640	109	8	210	210	NUM
ecletica-640	109	9	,	,	PUNCT
ecletica-640	109	10	1924	1924	NUM
ecletica-640	109	11	.	.	PUNCT
ecletica-640	110	1	[	[	PUNCT
ecletica-640	110	2	links	link	NOUN
ecletica-640	110	3	]	]	PUNCT
ecletica-640	110	4	7	7	NUM
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ecletica-640	110	6	,	,	PUNCT
ecletica-640	110	7	g.a	g.a	PROPN
ecletica-640	110	8	.	.	PROPN
ecletica-640	110	9	;	;	PUNCT
ecletica-640	110	10	singh	singh	PROPN
ecletica-640	110	11	,	,	PUNCT
ecletica-640	110	12	b.p	b.p	PROPN
ecletica-640	110	13	.	.	PROPN
ecletica-640	110	14	stable	stable	ADJ
ecletica-640	110	15	carbocations	carbocation	NOUN
ecletica-640	110	16	.	.	PUNCT
ecletica-640	111	1	a	a	DET
ecletica-640	111	2	-	-	PUNCT
ecletica-640	111	3	ethylenenaphthalenium	ethylenenaphthalenium	NOUN
ecletica-640	111	4	ions	ion	NOUN
ecletica-640	111	5	.	.	PUNCT
ecletica-640	112	1	j.	j.	PROPN
ecletica-640	112	2	am	am	PROPN
ecletica-640	112	3	.	.	PUNCT
ecletica-640	113	1	chem	chem	NOUN
ecletica-640	113	2	.	.	PUNCT
ecletica-640	114	1	soc	soc	PROPN
ecletica-640	114	2	.	.	PUNCT
ecletica-640	114	3	,	,	PUNCT
ecletica-640	114	4	v.104	v.104	PROPN
ecletica-640	114	5	,	,	PUNCT
ecletica-640	114	6	n.19	n.19	NOUN
ecletica-640	114	7	,	,	PUNCT
ecletica-640	114	8	p.5168	p.5168	NOUN
ecletica-640	114	9	-	-	PUNCT
ecletica-640	114	10	5172	5172	NUM
ecletica-640	114	11	,	,	PUNCT
ecletica-640	114	12	1982	1982	NUM
ecletica-640	114	13	.	.	PUNCT
ecletica-640	115	1	[	[	PUNCT
ecletica-640	115	2	links	link	NOUN
ecletica-640	115	3	]	]	PUNCT
ecletica-640	115	4	8	8	NUM
ecletica-640	115	5	overberger	overberger	NOUN
ecletica-640	115	6	,	,	PUNCT
ecletica-640	115	7	c.g	c.g	PROPN
ecletica-640	115	8	.	.	PROPN
ecletica-640	115	9	;	;	PUNCT
ecletica-640	115	10	kaye	kaye	PROPN
ecletica-640	115	11	,	,	PUNCT
ecletica-640	115	12	h.	h.	PROPN
ecletica-640	115	13	the	the	DET
ecletica-640	115	14	syntheses	synthesis	NOUN
ecletica-640	115	15	of	of	ADP
ecletica-640	115	16	some	some	DET
ecletica-640	115	17	optically	optically	ADV
ecletica-640	115	18	active	active	ADJ
ecletica-640	115	19	e	e	NOUN
ecletica-640	115	20	-	-	NOUN
ecletica-640	115	21	caprolactones	caprolactone	NOUN
ecletica-640	115	22	.	.	PUNCT
ecletica-640	116	1	j.	j.	PROPN
ecletica-640	116	2	am	am	PROPN
ecletica-640	116	3	.	.	PUNCT
ecletica-640	117	1	chem	chem	NOUN
ecletica-640	117	2	.	.	PUNCT
ecletica-640	118	1	soc	soc	PROPN
ecletica-640	118	2	.	.	PUNCT
ecletica-640	119	1	,	,	PUNCT
ecletica-640	119	2	v.89	v.89	X
ecletica-640	119	3	,	,	PUNCT
ecletica-640	119	4	n.22	n.22	PRON
ecletica-640	119	5	,	,	PUNCT
ecletica-640	119	6	p.5640	p.5640	NOUN
ecletica-640	119	7	-	-	PUNCT
ecletica-640	119	8	5646	5646	NUM
ecletica-640	119	9	,	,	PUNCT
ecletica-640	119	10	1967	1967	NUM
ecletica-640	119	11	.	.	PUNCT
ecletica-640	120	1	[	[	PUNCT
ecletica-640	120	2	links	link	NOUN
ecletica-640	120	3	]	]	PUNCT
ecletica-640	120	4	9	9	NUM
ecletica-640	120	5	paterson	paterson	NOUN
ecletica-640	120	6	,	,	PUNCT
ecletica-640	120	7	i.	i.	PROPN
ecletica-640	120	8	;	;	PUNCT
ecletica-640	120	9	fleming	fleming	PROPN
ecletica-640	120	10	,	,	PUNCT
ecletica-640	120	11	i.	i.	PROPN
ecletica-640	120	12	a	a	PROPN
ecletica-640	120	13	-	-	PUNCT
ecletica-640	120	14	methylenation	methylenation	NOUN
ecletica-640	120	15	of	of	ADP
ecletica-640	120	16	lactones	lactone	NOUN
ecletica-640	120	17	and	and	CCONJ
ecletica-640	120	18	esters	ester	NOUN
ecletica-640	120	19	zinc	zinc	NOUN
ecletica-640	120	20	bromide	bromide	NOUN
ecletica-640	120	21	-	-	PUNCT
ecletica-640	120	22	catalysed	catalyse	VERB
ecletica-640	120	23	phenylthiomethylation	phenylthiomethylation	NOUN
ecletica-640	120	24	of	of	ADP
ecletica-640	120	25	o	o	PROPN
ecletica-640	120	26	-	-	ADJ
ecletica-640	120	27	silylated	silylate	VERB
ecletica-640	120	28	enolates	enolate	NOUN
ecletica-640	120	29	.	.	PUNCT
ecletica-640	121	1	tetrahedron	tetrahedron	NOUN
ecletica-640	121	2	letters	letter	NOUN
ecletica-640	121	3	,	,	PUNCT
ecletica-640	121	4	n.11	n.11	NOUN
ecletica-640	121	5	,	,	PUNCT
ecletica-640	121	6	p.993	p.993	NOUN
ecletica-640	121	7	-	-	PUNCT
ecletica-640	121	8	994	994	NUM
ecletica-640	121	9	,	,	PUNCT
ecletica-640	121	10	1979	1979	NUM
ecletica-640	121	11	.	.	PUNCT
ecletica-640	122	1	[	[	PUNCT
ecletica-640	122	2	links	link	NOUN
ecletica-640	122	3	]	]	PUNCT
ecletica-640	122	4	10	10	NUM
ecletica-640	122	5	posner	posner	NOUN
ecletica-640	122	6	,	,	PUNCT
ecletica-640	122	7	g.h	g.h	PROPN
ecletica-640	122	8	.	.	PROPN
ecletica-640	122	9	substitution	substitution	NOUN
ecletica-640	122	10	reactions	reaction	NOUN
ecletica-640	122	11	using	use	VERB
ecletica-640	122	12	organocopper	organocopper	NOUN
ecletica-640	122	13	reagents	reagent	NOUN
ecletica-640	122	14	.	.	PUNCT
ecletica-640	123	1	organic	organic	ADJ
ecletica-640	123	2	reaction	reaction	NOUN
ecletica-640	123	3	,	,	PUNCT
ecletica-640	123	4	v.22	v.22	NOUN
ecletica-640	123	5	,	,	PUNCT
ecletica-640	123	6	p.253	p.253	NUM
ecletica-640	123	7	-	-	SYM
ecletica-640	123	8	400	400	NUM
ecletica-640	123	9	,	,	PUNCT
ecletica-640	123	10	1975	1975	NUM
ecletica-640	123	11	.	.	PUNCT
ecletica-640	124	1	[	[	PUNCT
ecletica-640	124	2	links	link	NOUN
ecletica-640	124	3	]	]	PUNCT
ecletica-640	124	4	11	11	NUM
ecletica-640	124	5	reetz	reetz	ADJ
ecletica-640	124	6	,	,	PUNCT
ecletica-640	124	7	m.t	m.t	PROPN
ecletica-640	124	8	.	.	PROPN
ecletica-640	124	9	lewis	lewis	PROPN
ecletica-640	124	10	acid	acid	PROPN
ecletica-640	124	11	induced	induce	VERB
ecletica-640	124	12	alfa	alfa	NOUN
ecletica-640	124	13	-	-	PUNCT
ecletica-640	124	14	alkylation	alkylation	NOUN
ecletica-640	124	15	of	of	ADP
ecletica-640	124	16	carbonyl	carbonyl	NOUN
ecletica-640	124	17	compounds	compound	NOUN
ecletica-640	124	18	.	.	PUNCT
ecletica-640	125	1	angew	angew	PROPN
ecletica-640	125	2	.	.	PUNCT
ecletica-640	126	1	chem	chem	PROPN
ecletica-640	126	2	.	.	PUNCT
ecletica-640	127	1	int	int	NOUN
ecletica-640	127	2	.	.	PUNCT
ecletica-640	128	1	ed	ed	NOUN
ecletica-640	128	2	.	.	PUNCT
ecletica-640	128	3	engl	engl	PROPN
ecletica-640	128	4	.	.	PROPN
ecletica-640	128	5	,	,	PUNCT
ecletica-640	129	1	v.21	v.21	PROPN
ecletica-640	129	2	,	,	PUNCT
ecletica-640	129	3	p.96	p.96	NOUN
ecletica-640	129	4	-	-	NOUN
ecletica-640	129	5	108	108	NUM
ecletica-640	129	6	,	,	PUNCT
ecletica-640	129	7	1982	1982	NUM
ecletica-640	129	8	.	.	PUNCT
ecletica-640	130	1	[	[	PUNCT
ecletica-640	130	2	links	link	NOUN
ecletica-640	130	3	]	]	PUNCT
ecletica-640	130	4	12	12	NUM
ecletica-640	130	5	skarzewski	skarzewski	PROPN
ecletica-640	130	6	,	,	PUNCT
ecletica-640	130	7	j.	j.	PROPN
ecletica-640	130	8	cerium	cerium	PROPN
ecletica-640	130	9	catalyzed	catalyze	VERB
ecletica-640	130	10	persulfate	persulfate	NOUN
ecletica-640	130	11	oxydation	oxydation	NOUN
ecletica-640	130	12	of	of	ADP
ecletica-640	130	13	polycyclic	polycyclic	ADJ
ecletica-640	130	14	aromatic	aromatic	ADJ
ecletica-640	130	15	hydrocarbons	hydrocarbon	NOUN
ecletica-640	130	16	to	to	ADP
ecletica-640	130	17	quinones	quinone	NOUN
ecletica-640	130	18	.	.	PUNCT
ecletica-640	131	1	tetrahedron	tetrahedron	PROPN
ecletica-640	131	2	,	,	PUNCT
ecletica-640	131	3	v.40	v.40	PROPN
ecletica-640	131	4	,	,	PUNCT
ecletica-640	131	5	n.23	n.23	NOUN
ecletica-640	131	6	,	,	PUNCT
ecletica-640	131	7	p.4997	p.4997	NOUN
ecletica-640	131	8	-	-	PUNCT
ecletica-640	131	9	5000	5000	NUM
ecletica-640	131	10	,	,	PUNCT
ecletica-640	131	11	1984	1984	NUM
ecletica-640	131	12	.	.	PUNCT
ecletica-640	132	1	[	[	PUNCT
ecletica-640	132	2	links	link	NOUN
ecletica-640	132	3	]	]	PUNCT
ecletica-640	132	4	13	13	NUM
ecletica-640	132	5	thomas	thomas	PROPN
ecletica-640	132	6	,	,	PUNCT
ecletica-640	132	7	a.f	a.f	PROPN
ecletica-640	132	8	.	.	PROPN
ecletica-640	132	9	;	;	PUNCT
ecletica-640	132	10	rey	rey	PROPN
ecletica-640	132	11	,	,	PUNCT
ecletica-640	132	12	f.	f.	PROPN
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ecletica-640	133	2	baeyer	baeyer	PROPN
ecletica-640	133	3	-	-	PUNCT
ecletica-640	133	4	villiger	villiger	NOUN
ecletica-640	133	5	reaction	reaction	NOUN
ecletica-640	133	6	of	of	ADP
ecletica-640	133	7	pinanones	pinanone	NOUN
ecletica-640	133	8	(	(	PUNCT
ecletica-640	133	9	bicyclo[3.1.1]heptanones	bicyclo[3.1.1]heptanone	NOUN
ecletica-640	133	10	)	)	PUNCT
ecletica-640	133	11	.	.	PUNCT
ecletica-640	134	1	tetrahedron	tetrahedron	NOUN
ecletica-640	134	2	,	,	PUNCT
ecletica-640	134	3	v.48	v.48	X
ecletica-640	134	4	,	,	PUNCT
ecletica-640	134	5	n.10	n.10	ADP
ecletica-640	134	6	,	,	PUNCT
ecletica-640	134	7	p.1927	p.1927	X
ecletica-640	134	8	-	-	SYM
ecletica-640	134	9	1942	1942	NUM
ecletica-640	134	10	,	,	PUNCT
ecletica-640	134	11	1992	1992	NUM
ecletica-640	134	12	.	.	PUNCT
ecletica-640	135	1	[	[	PUNCT
ecletica-640	135	2	links	link	NOUN
ecletica-640	135	3	]	]	PUNCT
ecletica-640	135	4	recebido	recebido	VERB
ecletica-640	135	5	em	em	PRON
ecletica-640	135	6	22.3.2001	22.3.2001	PROPN
ecletica-640	135	7	.	.	PUNCT
ecletica-640	136	1	aceito	aceito	PROPN
ecletica-640	136	2	em	em	PROPN
ecletica-640	136	3	19.4.2001	19.4.2001	PROPN
ecletica-640	136	4	.	.	PUNCT
ecletica-640	137	1	*	*	PUNCT
ecletica-640	137	2	universidade	universidade	PROPN
ecletica-640	137	3	de	de	PROPN
ecletica-640	137	4	cuiabá	cuiabá	PROPN
ecletica-640	137	5	dep	dep	PROPN
ecletica-640	137	6	.	.	PUNCT
ecletica-640	138	1	de	de	ADP
ecletica-640	138	2	farmácia	farmácia	PROPN
ecletica-640	138	3	e	e	PROPN
ecletica-640	138	4	bioquímica	bioquímica	PROPN
ecletica-640	138	5	.	.	PUNCT
ecletica-640	139	1	78015	78015	NUM
ecletica-640	139	2	-	-	PUNCT
ecletica-640	139	3	480	480	NUM
ecletica-640	139	4	cuiabá	cuiabá	PROPN
ecletica-640	139	5	mt	mt	PROPN
ecletica-640	139	6	brazil	brazil	PROPN
ecletica-640	139	7	.	.	PUNCT
ecletica-640	140	1	*	*	PUNCT
ecletica-640	140	2	*	*	PUNCT
ecletica-640	140	3	universidade	universidade	PROPN
ecletica-640	140	4	federal	federal	PROPN
ecletica-640	140	5	de	de	PROPN
ecletica-640	140	6	pernambuco	pernambuco	PROPN
ecletica-640	140	7	dep	dep	PROPN
ecletica-640	140	8	.	.	PUNCT
ecletica-640	140	9	de	de	PROPN
ecletica-640	140	10	química	química	PROPN
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ecletica-640	140	12	.	.	PUNCT
ecletica-640	141	1	50670	50670	NUM
ecletica-640	141	2	-	-	SYM
ecletica-640	141	3	901	901	NUM
ecletica-640	141	4	recife	recife	NOUN
ecletica-640	141	5	pe	pe	PROPN
ecletica-640	141	6	brazil	brazil	PROPN
ecletica-640	141	7	.	.	PUNCT
ecletica-640	142	1	http://www.scielo.br/scielo.php?script=sci_arttext&pid=s0100-46702001000100005&lng=en&nrm=iso&tlng=en#titulo	http://www.scielo.br/scielo.php?script=sci_arttext&pid=s0100-46702001000100005&lng=en&nrm=iso&tlng=en#titulo	PROPN
ecletica-640	142	2	http://www.scielo.br/scielo.php?script=sci_arttext&pid=s0100-46702001000100005&lng=en&nrm=iso&tlng=en#titulo	http://www.scielo.br/scielo.php?script=sci_arttext&pid=s0100-46702001000100005&lng=en&nrm=iso&tlng=en#titulo	PROPN
ecletica-640	142	3	javascript	javascript	NOUN
ecletica-640	142	4	:	:	PUNCT
ecletica-640	142	5	void(0	void(0	PROPN
ecletica-640	142	6	)	)	PUNCT
ecletica-640	142	7	;	;	PUNCT
ecletica-640	142	8	javascript	javascript	NOUN
ecletica-640	142	9	:	:	PUNCT
ecletica-640	142	10	void(0	void(0	PROPN
ecletica-640	142	11	)	)	PUNCT
ecletica-640	142	12	;	;	PUNCT
ecletica-640	142	13	javascript	javascript	NOUN
ecletica-640	142	14	:	:	PUNCT
ecletica-640	142	15	void(0	void(0	PROPN
ecletica-640	142	16	)	)	PUNCT
ecletica-640	142	17	;	;	PUNCT
ecletica-640	142	18	javascript	javascript	NOUN
ecletica-640	142	19	:	:	PUNCT
ecletica-640	142	20	void(0	void(0	PROPN
ecletica-640	142	21	)	)	PUNCT
ecletica-640	142	22	;	;	PUNCT
ecletica-640	142	23	javascript	javascript	NOUN
ecletica-640	142	24	:	:	PUNCT
ecletica-640	142	25	void(0	void(0	PROPN
ecletica-640	142	26	)	)	PUNCT
ecletica-640	142	27	;	;	PUNCT
ecletica-640	142	28	javascript	javascript	NOUN
ecletica-640	142	29	:	:	PUNCT
ecletica-640	142	30	void(0	void(0	PROPN
ecletica-640	142	31	)	)	PUNCT
ecletica-640	142	32	;	;	PUNCT
ecletica-640	142	33	javascript	javascript	NOUN
ecletica-640	142	34	:	:	PUNCT
ecletica-640	142	35	void(0	void(0	PROPN
ecletica-640	142	36	)	)	PUNCT
ecletica-640	142	37	;	;	PUNCT
ecletica-640	142	38	javascript	javascript	NOUN
ecletica-640	142	39	:	:	PUNCT
ecletica-640	142	40	void(0	void(0	PROPN
ecletica-640	142	41	)	)	PUNCT
ecletica-640	142	42	;	;	PUNCT
ecletica-640	142	43	javascript	javascript	NOUN
ecletica-640	142	44	:	:	PUNCT
ecletica-640	142	45	void(0	void(0	PROPN
ecletica-640	142	46	)	)	PUNCT
ecletica-640	142	47	;	;	PUNCT
ecletica-640	142	48	javascript	javascript	NOUN
ecletica-640	142	49	:	:	PUNCT
ecletica-640	142	50	void(0	void(0	PROPN
ecletica-640	142	51	)	)	PUNCT
ecletica-640	142	52	;	;	PUNCT
ecletica-640	142	53	eclética	eclética	PROPN
ecletica-640	142	54	química	química	PROPN
ecletica-640	142	55	print	print	PROPN
ecletica-640	142	56	 	 	SPACE
ecletica-640	142	57	version	version	PROPN
ecletica-640	142	58	 	 	SPACE
ecletica-640	142	59	issn	issn	PROPN
ecletica-640	142	60	0100	0100	NUM
ecletica-640	142	61	-	-	PUNCT
ecletica-640	142	62	4670on	4670on	NOUN
ecletica-640	142	63	-	-	PUNCT
ecletica-640	142	64	line	line	NOUN
ecletica-640	142	65	 	 	SPACE
ecletica-640	142	66	version	version	NOUN
ecletica-640	142	67	 	 	SPACE
ecletica-640	142	68	issn	issn	PROPN
ecletica-640	142	69	1678	1678	NUM
ecletica-640	142	70	-	-	SYM
ecletica-640	142	71	4618	4618	NUM
ecletica-640	142	72	eclet	eclet	NOUN
ecletica-640	142	73	.	.	PUNCT
ecletica-640	143	1	quím	quím	PROPN
ecletica-640	143	2	.	.	PUNCT
ecletica-640	143	3	 	 	SPACE
ecletica-640	144	1	vol.26	vol.26	ADJ
ecletica-640	144	2	  	  	SPACE
ecletica-640	144	3	são	são	PROPN
ecletica-640	144	4	paulo	paulo	PROPN
ecletica-640	144	5	  	  	SPACE
ecletica-640	144	6	2001	2001	NUM
ecletica-640	144	7	http://dx.doi.org/10.1590/s0100-46702001000100005	http://dx.doi.org/10.1590/s0100-46702001000100005	NOUN
ecletica-640	144	8	  	  	SPACE