id	author	title	date	pages	extension	mime	words	sentence	flesch	summary	cache	txt
eurjchem-1567	Khan, Maria Aqeel; Batool, Farhana; Khatoon, Asma; Sadiq, Rabia; Rahman, Sher; Basha, Fatima Zehra	Solvent-free protocol for the green synthesis of benzamide analogs of dibenzoazepine	2017	4	.pdf	application/pdf	3594	210	73	Entry Base Equivalence of 1: benzoyl chloride: base Solvent Temp (°C) Time (h) Yield (%) 1 DIPEA 1:1.4:1.4 THF 50 4.0 80 2 NEt3 1:3.4:1.2 DCM 25 1.8 93 3 NaHCO3 1:1.5:2 ‐ 140 0.5 60 4 NEt3 1:1:1.5 ‐ 25 24.0 Traces 5 NEt3 1:1:1.5 ‐ 50 24.0 54 6 NEt3 1:1:1.5 ‐ 100 2.0 76 7 NEt3 1:1:1.5 ‐ 120 0.3 82 8 NEt3 1:1.5:1.5 ‐ 120 0.3 98 (5'H‐Dibenzo[b, f]azepin‐5'‐yl)(phenyl)methanone (6): Color: Off white. MS (EI, m/z (%)): 297 (M+, 46).	cache/eurjchem-1567.pdf	txt/eurjchem-1567.txt