id	author	title	date	pages	extension	mime	words	sentence	flesch	summary	cache	txt
eurjchem-1602	Lo, Modou; Martínez, Andrea; Santalla, Hugo; Garrido, Fátima; Barry, Aliou Hamady; Gaye, Mohamed	Synthesis and X-ray crystallography of (1R,3aR,7aR)-1-((S)-1-((2R,5S)-5-(3-hydroxypentan-3-yl)tetrahydrofuran-2-yl)ethyl)-7a-methyloctahydro-4H-inden-4-one	2017	4	.pdf	application/pdf	2366	127	69	Synthesis of compound 1 To a solution of diol (2) (0.18 mmol) in CH2Cl2 (5 mL), pyridinium dichromate (PDC) (0.37 mmol) was added and the mixture stirred at room temperature for 12 h, then the solvent was evaporated and the residue was chromatographed on sılica gel using (10%, EtOAc:hexane, v:v) to afford ketone (1) (Scheme 1). 3. Results and discussion The compound 1 was prepared by a facile oxidation of compound 2 with pyridinium dichromate in dichloromethane (Scheme 1).	cache/eurjchem-1602.pdf	txt/eurjchem-1602.txt