id	author	title	date	pages	extension	mime	words	sentence	flesch	summary	cache	txt
eurjchem-438	Satpathy, Gouri; Tyagi, Yogesh Kumar; Gupta, Rajinder Kumar	A quick method for surveillance of 59 pesticide residues in fruits and vegetables using rapid three-dimensional gas chromatography (GC/MSD/µ-ECD/FPD) and LC/MS-MS	2011	11	.pdf	application/pdf	8753	296	52	[Results: mg/kg ± SD]. Name Beans n =2 Eggplant n = 18 Okra n =5 Radish n =2 Cauliflower n =11 Cabbage n =10 Capsicum n =4 Grapes n =8 Tomato n =11 Apple n =2 Formothion NDa ND ND ND ND 0.05 ND 0.04±0.04 ND ND Methyl Parathion ND ND ND ND ND ND 0.08±0.03 ND 0.12±0.05 ND Fenitrothion ND 0.33±0.17 0.41±0.16 ND 0.08±0.05 ND 0.16±0.17 ND 0.33±0.17 ND Malathion ND ND ND 0.22±0.08 0.22±0.12 ND ND ND 0.19±0.12 ND Fenthion ND 0.06±0.01 ND ND ND ND ND ND ND ND Parathion ND ND ND ND 0.11±0.04 ND ND ND ND ND Chlorpyriphos ND 0.13±0.27 0.33±0.17 ND 0.23±0.19 0.41±0.1 0.33±0.17 0.33±0.17 0.33±0.17 0.13±0.10 Captan ND ND 0.04±0.01 ND ND ND ND ND ND ND Endosulfan(total) ND ND ND ND ND ND ND 0.13±0.07 ND ND P, P DDE ND ND ND ND ND ND ND 0.019±0.01 ND ND P, P DDD ND ND ND ND ND 0.02±0.01 ND ND ND ND Ethion ND ND ND ND 0.12±0.01 0.07±0.01 ND ND 0.08±0.01 ND Phosalone ND ND 0.05±0.02 ND ND ND ND 0.03±0.01 ND ND Cypermathrin (total) ND 0.23±0.11 ND ND ND 0.14±0.04 ND ND ND 0.11±0.06 Fenvalerate (total) ND 0.07±0.17 0.33±0.17 ND ND ND ND ND ND ND Paraquat dichloride 0.03±0.01 ND ND ND ND ND ND 0.05±0.02 ND ND Carbaryl ND ND 0.05±0.02 ND 0.11±0.03 0.13±0.04 ND ND ND ND Carbendazim ND ND ND ND 0.08±0.01 ND ND 0.12±0.01 ND ND Benomyl 0.21±0.1 ND ND ND ND ND ND ND ND ND aND: Not detected. R.T. CAS # Compound Name Agilent AMDIS NIST ChemStation Amount (ppm) Match R.T. Diff sec. Reverse Match Hit Num. 2.7944 1113026 Omethoate ‐ 72 <20 79 2 2.8103 100185 Benzene, 1,4‐bis(1‐methylethyl)‐ ‐ ‐ <20 92 1 3.0534 623916 2‐Butenedioic acid (E)‐, diethyl ester ‐ ‐ <20 96 1 3.5892 7786‐34‐7 Dichlorvos 0.077 95 <20 92 2 3.6479 90120 Naphthalene, 1‐methyl‐ ‐ ‐ <20 82 1 3.7969 717748 Benzene, 1,3,5‐tris(1‐methylethyl)‐ ‐ ‐ <20 79 1 3.9935 2040053 2,6‐Dichloroacetophenone ‐ ‐ <20 80 1 4.3143 2032657 Methiocarb ‐ 86 <20 ‐ ‐ 4.5399 28839498 1H‐Isoindole‐1,3(2H)‐dione, 4,5,6,7‐tetrahydro‐2‐methyl ‐ ‐ <20 85 1 4.6620 0000 l‐Alanine, N‐(2,6‐difluorobenzoyl)‐, hexyl ester ‐ ‐ <20 83 1 4.7027 626437 3,5‐Dichloroaniline ‐ 98 <20 ‐ ‐ 4.7027 95761 Benzenamine, 3,4‐dichloro‐ ‐ ‐ <20 95 1 5.0441 27813214 Tetrahydrophthalimide, cis‐1,2,3,6‐ ‐ 95 <20 ‐ ‐ 5.0451 6923224 Monocrotophos 0.081 97 <20 94 1 5.0732 6108107 BHC epsilon isomer 0.098 86 <20 ‐ ‐ 5.0732 28903244 Cyclohexene, pentachloro‐ ‐ ‐ <20 92 1 5.2185 90153 1‐naphthalenol 0.079 98 <20 93 1 5.5107 4185824 Phosphoric acid, dimethyl 1‐methylethenyl ester ‐ ‐ <20 72 1 5.7004 298022 Phorate 0.103 90 <20 89 2 5.7152 39515510 Benzaldehyde, 3‐phenoxy‐ ‐ ‐ <20 92 1 5.8029 319846 BHC alpha isomer 0.080 99 <20 93 2 5.8294 640153 Thiometon 0.083 88 <20 92 2 5.8801 100027 4‐Nitrophenol 0.091 88 <20 86 2 6.1380 20925853 Benzonitrile, pentachloro‐ ‐ ‐ <20 81 1 6.1639 319857 BHC beta isomer 0.093 99 <20 82 1 6.3341 60515 Dimethoate 0.088 95 <20 91 2 6.6189 84695 Diisobutyl phthalate ‐ 90 <20 90 1 6.816 58899 Lindane 0.086 88 <20 76 1 6.1639 319857 BHC delta isomer 0.096 90 <20 82 1 6.8197 1897456 Chlorothalonil 0.101 96 <20 90 2 6.9196 34256821 Acetochlor 0.084 72 <20 71 1 6.9344 95250 Chlorzoxazone ‐ ‐ <20 73 1 6.952 319868 BHC delta isomer 0.103 83 <20 94 1 7.006 1897456 Chlorthalonil 0.099 81 <20 91 1 7.0270 2540821 Formothion 0.105 90 <20 81 2 7.170 298000 Methyl parathion 0.077 91 <20 92 2 7.227 76448 Heptachlor 0.087 98 <20 91 1 7.3033 84742 Di‐n‐butylphthalate ‐ 84 <20 84 1 7.5300 122145 Fenitrothion 0.104 89 <20 85 1 7.5934 309002 Aldrin 0.086 92 <20 88 2 7.6130 121755 Malathion 0.092 93 <20 92 2 7.6606 85290 2,4'‐Dichlorobenzophenone (2,4'‐Dicofol decom.product) ‐ 85 <20 90 2 7.717 55389 Fenthion 0.081 92 <20 87 1 7.884 56382 Parathion 0.079 94 <20 90 1 8.018 2921882 Chloropyriphos 0.100 91 <20 87 1 8.072 43121433 Triadimefon 0.107 88 <20 79 1 8.118 470906 Chlorfenvinfos alpha 0.096 89 <20 77 1 8.209 133062 Captan 0.092 82 <20 73 1 8.221 470906 Chlorfenvinfos beta 0.082 91 <20 76 1 8.249 13593038 Quinalphos 0.087 88 <20 71 1 8.2836 3424826 o,p'‐DDE 0.093 97 <20 92 2 8.302 57749 Chlordane‐I 0.105 77 <20 78 1 8.314 18181709 Jodfenphos 0.099 82 <20 76 1 8.415 57749 Chlordane ‐ II 0.089 83 <20 74 ‐ 8.4210 959988 Endosulfan (alpha isomer) 0.091 98 <20 72 1 8.5853 5103742 trans‐Chlordane 0.081 82 <20 78 2 8.6810 39765805 Nonachlor, trans‐ 0.079 83 <20 83 2 8.7486 15972608 Alachlor 0.102 73 <20 ‐ ‐ 8.7486 23184669 Butachlor 0.106 97 <20 91 1 8.8031 72559 p,p'‐DDE 0.098 92 <20 89 2 8.9288 60571 Dieldrin 0.104 96 <20 92 2 9.0535 66870891 p‐Tolylpentamethyl‐disiloxane ‐ ‐ <20 77 1 9.068 41198087 Profenofos 0.092 82 <20 76 1 9.520 72208 Endrin 0.102 87 <20 79 1 9.6428 510156 Chlorobenzilate 0.104 96 <20 93 2 9.7786 33213659 Endosulfan (beta isomer) 0.082 78 <20 76 1 9.8177 53190 o,p'‐DDD 0.088 98 <20 94 2 9.826 72548 P, P DDD 0.098 88 <20 77 1 9.9324 563122 Ethion 0.103 95 <20 89 2 10.311 789026 Triazophos 0.093 97 <20 88 1 10.7732 1031078 Endosulfan sulfate 0.092 95 <20 85 1 10.930 2425061 Captafol 0.085 97 <20 76 1 11.6235 117817 Bis(2‐ethylhexyl)phthalate ‐ 73 <20 ‐ ‐ 11.6235 4376209 1,2‐Benzenedicarboxylic acid, mono(2‐ethylhexyl) ester ‐ ‐ <20 78 1 12.2037 2310170 Phosalone 0.098 96 <20 90 1 12.742 52645531 Permethrin ‐ I 0.087 93 <20 84 1 12.973 52645531 Permathrin ‐ II 0.091 96 <20 97 1 13.891 52315078 Cypermethrin I 0.105 73 <20 76 1 14.1648 52315078 Cypermethrin II 0.093 81 <20 84 1 14.7414 66230044 Esfenvalerate 0.080 89 <20 91 1 14.9620 51630581 Fenvalerate I 0.106 87 <20 76 1 Satpathy et al. / European Journal of Chemistry 2 (4) (2011) 524‐534 531 Figure 1. Linearity graph of paraquat dichloride for 10 levels.	cache/eurjchem-438.pdf	txt/eurjchem-438.txt