id	author	title	date	pages	extension	mime	words	sentence	flesch	summary	cache	txt
eurjchem-768	Kumar, Rathod Aravind; Kashanna, Jajula; Jangili, Paramesh; Das, Biswanath	A simple stereoselective synthesis of (+)-[6]-gingerdiol	2013	4	.pdf	application/pdf	3490	183	76	4‐(tert‐Butyl dimethyl silyloxy)‐3‐methoxy benzaldehyde (5) To a stirred solution of compound 4 (1.0 g, 6.57 mmol) and imidazole (1.78 g, 26.28 mmol) in dry DCM (15 mL) was added tert‐butyl chloro (dimethyl) silane (TBS‐Cl) (1.98 g, 13.15 mmol) slowly at 0 °C. Found: C, 66.09; H, 9.18%. 2.2.8. (4R,6R)‐4‐(4‐(tert‐butyl dimethyl silyloxy)‐3‐methoxy phenethyl)‐6‐(iodomethyl)‐1,3‐dioxan‐2‐one (10) A mixture of compound 9 (0.060 g, 0.137 mmol) and I2 (0.034 g, 1.374 mmol) in 10 mL of dry MeCN was stirred mechanically under N2 atmosphere at ‐20 oC for 6 h.	cache/eurjchem-768.pdf	txt/eurjchem-768.txt