id	author	title	date	pages	extension	mime	words	sentence	flesch	summary	cache	txt
eurjchem-917	Manneganti, Vijay; Rachapudi, Badari Narayana Prasad; Bethala, Lakshmi Anu Prabhavathi Devi	SO3H-Carbon derived from glycerol: An efficient and recyclable catalyst for smooth and regioselective azidolysis of oxiranes in water	2014	4	.pdf	application/pdf	3068	210	70	3. Results and discussion Initially, different solvents like CH3COCH3, CH2Cl2, THF, CH3CN, DMF and H2O were screened for the azidolysis of styrene oxide by treating with 1.2 mmol of sodium azide in presence of 10 wt% of catalyst at reflux temperatures. It was investigated to optimize the reaction conditions like H2O content (0.5 to 2 mL), amount of the catalyst (2 to 10 wt% of oxirane) and sodium azide (1 to 2 mmol) for complete azidolysis of styrene oxide (1 mmol) to the corresponding azidohydrin at 90 C. From this study, the optimum conditions were found to be 1.2 mmol of NaN3 and 2 wt% of catalyst in 1 mL of water at 90 °C for 0.5 h.	cache/eurjchem-917.pdf	txt/eurjchem-917.txt