id	sid	tid	token	lemma	pos
eurjchem-1000	1	1	untitled	untitle	VERB
eurjchem-1000	1	2	european	european	PROPN
eurjchem-1000	1	3	journal	journal	PROPN
eurjchem-1000	1	4	of	of	ADP
eurjchem-1000	1	5	chemistry	chemistry	NOUN
eurjchem-1000	1	6	5	5	NUM
eurjchem-1000	1	7	(	(	PUNCT
eurjchem-1000	1	8	2	2	NUM
eurjchem-1000	1	9	)	)	PUNCT
eurjchem-1000	1	10	(	(	PUNCT
eurjchem-1000	1	11	2014	2014	NUM
eurjchem-1000	1	12	)	)	PUNCT
eurjchem-1000	1	13	241‐246	241‐246	NUM
eurjchem-1000	1	14	european	european	ADJ
eurjchem-1000	1	15	journal	journal	PROPN
eurjchem-1000	1	16	of	of	ADP
eurjchem-1000	1	17	chemistry	chemistry	NOUN
eurjchem-1000	1	18	issn	issn	PROPN
eurjchem-1000	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-1000	1	20	(	(	PUNCT
eurjchem-1000	1	21	print	print	NOUN
eurjchem-1000	1	22	)	)	PUNCT
eurjchem-1000	1	23	/	/	SYM
eurjchem-1000	1	24	issn	issn	PROPN
eurjchem-1000	1	25	2153‐2257	2153‐2257	NUM
eurjchem-1000	1	26	(	(	PUNCT
eurjchem-1000	1	27	online	online	ADJ
eurjchem-1000	1	28	)	)	PUNCT
eurjchem-1000	1	29			NOUN
eurjchem-1000	1	30	2014	2014	NUM
eurjchem-1000	2	1	eurjchem	eurjchem	PROPN
eurjchem-1000	2	2	publishing	publish	VERB
eurjchem-1000	2	3	‐	‐	NOUN
eurjchem-1000	2	4	printed	print	VERB
eurjchem-1000	2	5	in	in	ADP
eurjchem-1000	2	6	the	the	DET
eurjchem-1000	2	7	usa	usa	PROPN
eurjchem-1000	2	8	http://dx.doi.org/10.5155/eurjchem.5.2.241‐246.1000	http://dx.doi.org/10.5155/eurjchem.5.2.241‐246.1000	PROPN
eurjchem-1000	2	9	european	european	PROPN
eurjchem-1000	2	10	journal	journal	PROPN
eurjchem-1000	2	11	of	of	ADP
eurjchem-1000	2	12	chemistry	chemistry	PROPN
eurjchem-1000	2	13	journal	journal	PROPN
eurjchem-1000	2	14	homepage	homepage	NOUN
eurjchem-1000	2	15	:	:	PUNCT
eurjchem-1000	2	16	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1000	2	17	a	a	DET
eurjchem-1000	2	18	new	new	ADJ
eurjchem-1000	2	19	validated	validate	VERB
eurjchem-1000	2	20	bio‐analytical	bio‐analytical	ADJ
eurjchem-1000	2	21	liquid	liquid	ADJ
eurjchem-1000	2	22	chromatographic‐tandem	chromatographic‐tandem	NOUN
eurjchem-1000	2	23	mass	mass	NOUN
eurjchem-1000	2	24	spectrometric	spectrometric	NOUN
eurjchem-1000	2	25	(	(	PUNCT
eurjchem-1000	2	26	lc‐ms	lc‐ms	NOUN
eurjchem-1000	2	27	/	/	SYM
eurjchem-1000	2	28	ms	ms	PROPN
eurjchem-1000	2	29	)	)	PUNCT
eurjchem-1000	2	30	method	method	NOUN
eurjchem-1000	2	31	for	for	ADP
eurjchem-1000	2	32	the	the	DET
eurjchem-1000	2	33	quantification	quantification	NOUN
eurjchem-1000	2	34	of	of	ADP
eurjchem-1000	2	35	azithromycin	azithromycin	PROPN
eurjchem-1000	2	36	in	in	ADP
eurjchem-1000	2	37	human	human	ADJ
eurjchem-1000	2	38	plasma	plasma	NOUN
eurjchem-1000	2	39	kareem	kareem	PROPN
eurjchem-1000	2	40	mahmoud	mahmoud	PROPN
eurjchem-1000	2	41	younes	younes	PROPN
eurjchem-1000	2	42	a	a	PRON
eurjchem-1000	2	43	,	,	PUNCT
eurjchem-1000	2	44	*	*	PUNCT
eurjchem-1000	2	45	and	and	CCONJ
eurjchem-1000	2	46	ehab	ehab	PROPN
eurjchem-1000	2	47	farouk	farouk	PROPN
eurjchem-1000	2	48	el‐kady	el‐kady	PROPN
eurjchem-1000	2	49	b	b	PROPN
eurjchem-1000	2	50	a	a	DET
eurjchem-1000	2	51	analytical	analytical	ADJ
eurjchem-1000	2	52	chemistry	chemistry	NOUN
eurjchem-1000	2	53	department	department	NOUN
eurjchem-1000	2	54	,	,	PUNCT
eurjchem-1000	2	55	faculty	faculty	NOUN
eurjchem-1000	2	56	of	of	ADP
eurjchem-1000	2	57	pharmacy	pharmacy	NOUN
eurjchem-1000	2	58	,	,	PUNCT
eurjchem-1000	2	59	cairo	cairo	PROPN
eurjchem-1000	2	60	university	university	PROPN
eurjchem-1000	2	61	,	,	PUNCT
eurjchem-1000	2	62	cairo	cairo	PROPN
eurjchem-1000	2	63	,	,	PUNCT
eurjchem-1000	2	64	et‐11562	et‐11562	PROPN
eurjchem-1000	2	65	,	,	PUNCT
eurjchem-1000	2	66	egypt	egypt	PROPN
eurjchem-1000	2	67	b	b	PROPN
eurjchem-1000	2	68	pharmaceutical	pharmaceutical	ADJ
eurjchem-1000	2	69	chemistry	chemistry	NOUN
eurjchem-1000	2	70	department	department	NOUN
eurjchem-1000	2	71	,	,	PUNCT
eurjchem-1000	2	72	faculty	faculty	NOUN
eurjchem-1000	2	73	of	of	ADP
eurjchem-1000	2	74	pharmacy	pharmacy	NOUN
eurjchem-1000	2	75	,	,	PUNCT
eurjchem-1000	2	76	cairo	cairo	PROPN
eurjchem-1000	2	77	university	university	PROPN
eurjchem-1000	2	78	,	,	PUNCT
eurjchem-1000	2	79	cairo	cairo	PROPN
eurjchem-1000	2	80	,	,	PUNCT
eurjchem-1000	2	81	et‐11562	et‐11562	PROPN
eurjchem-1000	2	82	,	,	PUNCT
eurjchem-1000	2	83	egypt	egypt	PROPN
eurjchem-1000	2	84	*	*	PUNCT
eurjchem-1000	2	85	corresponding	correspond	VERB
eurjchem-1000	2	86	author	author	NOUN
eurjchem-1000	2	87	at	at	ADP
eurjchem-1000	2	88	:	:	PUNCT
eurjchem-1000	2	89	analytical	analytical	ADJ
eurjchem-1000	2	90	chemistry	chemistry	NOUN
eurjchem-1000	2	91	department	department	NOUN
eurjchem-1000	2	92	,	,	PUNCT
eurjchem-1000	2	93	faculty	faculty	NOUN
eurjchem-1000	2	94	of	of	ADP
eurjchem-1000	2	95	pharmacy	pharmacy	NOUN
eurjchem-1000	2	96	,	,	PUNCT
eurjchem-1000	2	97	cairo	cairo	PROPN
eurjchem-1000	2	98	university	university	PROPN
eurjchem-1000	2	99	,	,	PUNCT
eurjchem-1000	2	100	cairo	cairo	PROPN
eurjchem-1000	2	101	,	,	PUNCT
eurjchem-1000	2	102	et‐11562	et‐11562	PROPN
eurjchem-1000	2	103	,	,	PUNCT
eurjchem-1000	2	104	egypt	egypt	PROPN
eurjchem-1000	2	105	.	.	PUNCT
eurjchem-1000	3	1	tel	tel	PROPN
eurjchem-1000	3	2	.	.	PUNCT
eurjchem-1000	3	3	:	:	PUNCT
eurjchem-1000	4	1	+2.02.01141731229	+2.02.01141731229	X
eurjchem-1000	4	2	.	.	PUNCT
eurjchem-1000	5	1	fax	fax	NOUN
eurjchem-1000	5	2	:	:	PUNCT
eurjchem-1000	5	3	+2.02.23628246	+2.02.23628246	PROPN
eurjchem-1000	5	4	.	.	PUNCT
eurjchem-1000	5	5	e‐mail	e‐mail	PUNCT
eurjchem-1000	6	1	address	address	NOUN
eurjchem-1000	6	2	:	:	PUNCT
eurjchem-1000	6	3	kareemchem99@yahoo.com	kareemchem99@yahoo.com	PROPN
eurjchem-1000	6	4	(	(	PUNCT
eurjchem-1000	6	5	k.m	k.m	PROPN
eurjchem-1000	6	6	.	.	PROPN
eurjchem-1000	6	7	younes	younes	PROPN
eurjchem-1000	6	8	)	)	PUNCT
eurjchem-1000	6	9	.	.	PUNCT
eurjchem-1000	7	1	article	article	NOUN
eurjchem-1000	7	2	information	information	PROPN
eurjchem-1000	7	3	abstract	abstract	ADJ
eurjchem-1000	7	4	doi	doi	NOUN
eurjchem-1000	7	5	:	:	PUNCT
eurjchem-1000	7	6	10.5155	10.5155	NUM
eurjchem-1000	7	7	/	/	SYM
eurjchem-1000	7	8	eurjchem.5.2.241‐246.1000	eurjchem.5.2.241‐246.1000	PRON
eurjchem-1000	7	9	received	receive	VERB
eurjchem-1000	7	10	:	:	PUNCT
eurjchem-1000	7	11	09	09	NUM
eurjchem-1000	7	12	december	december	PROPN
eurjchem-1000	7	13	2013	2013	NUM
eurjchem-1000	7	14	received	receive	VERB
eurjchem-1000	7	15	in	in	ADP
eurjchem-1000	7	16	revised	revise	VERB
eurjchem-1000	7	17	form	form	NOUN
eurjchem-1000	7	18	:	:	PUNCT
eurjchem-1000	7	19	26	26	NUM
eurjchem-1000	7	20	december	december	PROPN
eurjchem-1000	7	21	2013	2013	NUM
eurjchem-1000	7	22	accepted	accept	VERB
eurjchem-1000	7	23	:	:	PUNCT
eurjchem-1000	7	24	26	26	NUM
eurjchem-1000	7	25	december	december	PROPN
eurjchem-1000	7	26	2013	2013	NUM
eurjchem-1000	7	27	online	online	NOUN
eurjchem-1000	7	28	:	:	PUNCT
eurjchem-1000	7	29	30	30	NUM
eurjchem-1000	7	30	june	june	PROPN
eurjchem-1000	7	31	2014	2014	NUM
eurjchem-1000	7	32	keywords	keyword	VERB
eurjchem-1000	7	33	a	a	DET
eurjchem-1000	7	34	simple	simple	ADJ
eurjchem-1000	7	35	,	,	PUNCT
eurjchem-1000	7	36	rapid	rapid	ADJ
eurjchem-1000	7	37	and	and	CCONJ
eurjchem-1000	7	38	sensitive	sensitive	ADJ
eurjchem-1000	7	39	lc‐ms	lc‐ms	AUX
eurjchem-1000	7	40	/	/	SYM
eurjchem-1000	7	41	ms	ms	PROPN
eurjchem-1000	7	42	method	method	NOUN
eurjchem-1000	7	43	was	be	AUX
eurjchem-1000	7	44	developed	develop	VERB
eurjchem-1000	7	45	and	and	CCONJ
eurjchem-1000	7	46	validated	validate	VERB
eurjchem-1000	7	47	for	for	ADP
eurjchem-1000	7	48	the	the	DET
eurjchem-1000	7	49	quantification	quantification	NOUN
eurjchem-1000	7	50	of	of	ADP
eurjchem-1000	7	51	azithromycin	azithromycin	PROPN
eurjchem-1000	7	52	(	(	PUNCT
eurjchem-1000	7	53	azi	azi	PROPN
eurjchem-1000	7	54	)	)	PUNCT
eurjchem-1000	7	55	in	in	ADP
eurjchem-1000	7	56	human	human	ADJ
eurjchem-1000	7	57	plasma	plasma	NOUN
eurjchem-1000	7	58	.	.	PUNCT
eurjchem-1000	8	1	sildenafil	sildenafil	PROPN
eurjchem-1000	8	2	citrate	citrate	PROPN
eurjchem-1000	8	3	was	be	AUX
eurjchem-1000	8	4	used	use	VERB
eurjchem-1000	8	5	as	as	ADP
eurjchem-1000	8	6	an	an	DET
eurjchem-1000	8	7	internal	internal	ADJ
eurjchem-1000	8	8	standard	standard	NOUN
eurjchem-1000	8	9	.	.	PUNCT
eurjchem-1000	9	1	the	the	DET
eurjchem-1000	9	2	analytes	analyte	NOUN
eurjchem-1000	9	3	were	be	AUX
eurjchem-1000	9	4	extracted	extract	VERB
eurjchem-1000	9	5	from	from	ADP
eurjchem-1000	9	6	human	human	ADJ
eurjchem-1000	9	7	plasma	plasma	NOUN
eurjchem-1000	9	8	samples	sample	NOUN
eurjchem-1000	9	9	by	by	ADP
eurjchem-1000	9	10	liquid‐liquid	liquid‐liquid	ADJ
eurjchem-1000	9	11	extraction	extraction	NOUN
eurjchem-1000	9	12	technique	technique	NOUN
eurjchem-1000	9	13	.	.	PUNCT
eurjchem-1000	10	1	the	the	DET
eurjchem-1000	10	2	reconstituted	reconstitute	VERB
eurjchem-1000	10	3	samples	sample	NOUN
eurjchem-1000	10	4	were	be	AUX
eurjchem-1000	10	5	chromatographed	chromatographe	VERB
eurjchem-1000	10	6	on	on	ADP
eurjchem-1000	10	7	a	a	DET
eurjchem-1000	10	8	reversed	reversed	ADJ
eurjchem-1000	10	9	‐	‐	ADJ
eurjchem-1000	10	10	phase	phase	NOUN
eurjchem-1000	10	11	column	column	NOUN
eurjchem-1000	10	12	c18	c18	NOUN
eurjchem-1000	10	13	,	,	PUNCT
eurjchem-1000	10	14	50	50	NUM
eurjchem-1000	10	15	×	×	NOUN
eurjchem-1000	10	16	2.1	2.1	NUM
eurjchem-1000	10	17	mm	mm	NOUN
eurjchem-1000	10	18	,	,	PUNCT
eurjchem-1000	10	19	5	5	NUM
eurjchem-1000	10	20	µm	µm	NOUN
eurjchem-1000	10	21	from	from	ADP
eurjchem-1000	10	22	waters	water	NOUN
eurjchem-1000	10	23	,	,	PUNCT
eurjchem-1000	10	24	by	by	ADP
eurjchem-1000	10	25	using	use	VERB
eurjchem-1000	10	26	a	a	DET
eurjchem-1000	10	27	80:20	80:20	NUM
eurjchem-1000	10	28	(	(	PUNCT
eurjchem-1000	10	29	v	v	NOUN
eurjchem-1000	10	30	:	:	PUNCT
eurjchem-1000	10	31	v	v	NOUN
eurjchem-1000	10	32	)	)	PUNCT
eurjchem-1000	10	33	mixture	mixture	NOUN
eurjchem-1000	10	34	of	of	ADP
eurjchem-1000	10	35	acetonitrile	acetonitrile	NOUN
eurjchem-1000	10	36	and	and	CCONJ
eurjchem-1000	10	37	0.1	0.1	NUM
eurjchem-1000	10	38	%	%	NOUN
eurjchem-1000	10	39	formic	formic	NOUN
eurjchem-1000	10	40	acid	acid	NOUN
eurjchem-1000	10	41	in	in	ADP
eurjchem-1000	10	42	water	water	NOUN
eurjchem-1000	10	43	as	as	ADP
eurjchem-1000	10	44	the	the	DET
eurjchem-1000	10	45	mobile	mobile	ADJ
eurjchem-1000	10	46	phase	phase	NOUN
eurjchem-1000	10	47	at	at	ADP
eurjchem-1000	10	48	a	a	DET
eurjchem-1000	10	49	flow	flow	NOUN
eurjchem-1000	10	50	rate	rate	NOUN
eurjchem-1000	10	51	of	of	ADP
eurjchem-1000	10	52	0.5	0.5	NUM
eurjchem-1000	10	53	ml	ml	NOUN
eurjchem-1000	10	54	/	/	SYM
eurjchem-1000	10	55	min	min	NOUN
eurjchem-1000	10	56	.	.	PUNCT
eurjchem-1000	11	1	the	the	DET
eurjchem-1000	11	2	calibration	calibration	NOUN
eurjchem-1000	11	3	curve	curve	NOUN
eurjchem-1000	11	4	was	be	AUX
eurjchem-1000	11	5	linear	linear	ADJ
eurjchem-1000	11	6	(	(	PUNCT
eurjchem-1000	11	7	r2	r2	PROPN
eurjchem-1000	11	8	>	>	X
eurjchem-1000	11	9	0.99	0.99	NUM
eurjchem-1000	11	10	)	)	PUNCT
eurjchem-1000	11	11	over	over	ADP
eurjchem-1000	11	12	the	the	DET
eurjchem-1000	11	13	concentration	concentration	NOUN
eurjchem-1000	11	14	range	range	NOUN
eurjchem-1000	11	15	of	of	ADP
eurjchem-1000	11	16	5.0‐1500.0	5.0‐1500.0	NUM
eurjchem-1000	11	17	ng	ng	NOUN
eurjchem-1000	11	18	/	/	SYM
eurjchem-1000	11	19	ml	ml	PROPN
eurjchem-1000	11	20	.	.	PUNCT
eurjchem-1000	12	1	the	the	DET
eurjchem-1000	12	2	results	result	NOUN
eurjchem-1000	12	3	of	of	ADP
eurjchem-1000	12	4	the	the	DET
eurjchem-1000	12	5	intra‐	intra‐	PROPN
eurjchem-1000	12	6	and	and	CCONJ
eurjchem-1000	12	7	inter‐day	inter‐day	PROPN
eurjchem-1000	12	8	precision	precision	NOUN
eurjchem-1000	12	9	and	and	CCONJ
eurjchem-1000	12	10	accuracy	accuracy	NOUN
eurjchem-1000	12	11	studies	study	NOUN
eurjchem-1000	12	12	were	be	AUX
eurjchem-1000	12	13	within	within	ADP
eurjchem-1000	12	14	the	the	DET
eurjchem-1000	12	15	acceptable	acceptable	ADJ
eurjchem-1000	12	16	limits	limit	NOUN
eurjchem-1000	12	17	.	.	PUNCT
eurjchem-1000	13	1	a	a	DET
eurjchem-1000	13	2	run	run	ADJ
eurjchem-1000	13	3	time	time	NOUN
eurjchem-1000	13	4	of	of	ADP
eurjchem-1000	13	5	0.5	0.5	NUM
eurjchem-1000	13	6	min	min	NOUN
eurjchem-1000	13	7	for	for	ADP
eurjchem-1000	13	8	each	each	DET
eurjchem-1000	13	9	sample	sample	NOUN
eurjchem-1000	13	10	made	make	VERB
eurjchem-1000	13	11	it	it	PRON
eurjchem-1000	13	12	possible	possible	ADJ
eurjchem-1000	13	13	to	to	PART
eurjchem-1000	13	14	analyze	analyze	VERB
eurjchem-1000	13	15	more	more	ADJ
eurjchem-1000	13	16	than	than	ADP
eurjchem-1000	13	17	400	400	NUM
eurjchem-1000	13	18	plasma	plasma	NOUN
eurjchem-1000	13	19	samples	sample	NOUN
eurjchem-1000	13	20	per	per	ADP
eurjchem-1000	13	21	day	day	NOUN
eurjchem-1000	13	22	.	.	PUNCT
eurjchem-1000	14	1	azithromycin	azithromycin	PROPN
eurjchem-1000	14	2	sildenafil	sildenafil	PROPN
eurjchem-1000	14	3	citrate	citrate	PROPN
eurjchem-1000	14	4	internal	internal	PROPN
eurjchem-1000	14	5	standard	standard	PROPN
eurjchem-1000	14	6	mass	mass	ADJ
eurjchem-1000	14	7	spectrometry	spectrometry	NOUN
eurjchem-1000	14	8	liquid‐liquid	liquid‐liquid	NOUN
eurjchem-1000	14	9	extraction	extraction	NOUN
eurjchem-1000	14	10	liquid	liquid	ADJ
eurjchem-1000	14	11	chromatography	chromatography	NOUN
eurjchem-1000	14	12	1	1	NUM
eurjchem-1000	14	13	.	.	PUNCT
eurjchem-1000	15	1	introduction	introduction	NOUN
eurjchem-1000	15	2	azithromycin	azithromycin	PROPN
eurjchem-1000	15	3	designated	designate	VERB
eurjchem-1000	15	4	chemically	chemically	ADV
eurjchem-1000	15	5	as	as	ADP
eurjchem-1000	15	6	2r,3s,4r,5r,8r,10r	2r,3s,4r,5r,8r,10r	NUM
eurjchem-1000	15	7	,	,	PUNCT
eurjchem-1000	15	8	11r,12s,13s,14r)‐2‐ethyl‐3,4,10‐trihydroxy	11r,12s,13s,14r)‐2‐ethyl‐3,4,10‐trihydroxy	NUM
eurjchem-1000	15	9	3,5,6,8,10,12,14‐	3,5,6,8,10,12,14‐	NUM
eurjchem-1000	15	10	heptamethyl‐15‐oxo‐11‐{[3,4,6‐trideoxy‐3‐(dimethylamino)‐β‐	heptamethyl‐15‐oxo‐11‐{[3,4,6‐trideoxy‐3‐(dimethylamino)‐β‐	PROPN
eurjchem-1000	15	11	d‐xylo‐]oxy}‐1‐oxa‐6‐azacyclopentadec‐13‐yl2,6‐dideoxy‐3‐c	d‐xylo‐]oxy}‐1‐oxa‐6‐azacyclopentadec‐13‐yl2,6‐dideoxy‐3‐c	NOUN
eurjchem-1000	15	12	methyl‐3‐o‐methyl‐α‐l‐ribo‐hexopyranoside	methyl‐3‐o‐methyl‐α‐l‐ribo‐hexopyranoside	NOUN
eurjchem-1000	16	1	[	[	X
eurjchem-1000	16	2	1	1	X
eurjchem-1000	16	3	]	]	PUNCT
eurjchem-1000	16	4	(	(	PUNCT
eurjchem-1000	16	5	figure	figure	NOUN
eurjchem-1000	16	6	1	1	NUM
eurjchem-1000	16	7	)	)	PUNCT
eurjchem-1000	16	8	is	be	AUX
eurjchem-1000	16	9	a	a	DET
eurjchem-1000	16	10	semi‐synthetic	semi‐synthetic	ADJ
eurjchem-1000	16	11	macrolide	macrolide	ADJ
eurjchem-1000	16	12	antibiotic	antibiotic	NOUN
eurjchem-1000	16	13	of	of	ADP
eurjchem-1000	16	14	the	the	DET
eurjchem-1000	16	15	azalide	azalide	ADJ
eurjchem-1000	16	16	class	class	NOUN
eurjchem-1000	16	17	.	.	PUNCT
eurjchem-1000	17	1	azithromycin	azithromycin	PROPN
eurjchem-1000	17	2	inhibits	inhibit	VERB
eurjchem-1000	17	3	bacterial	bacterial	ADJ
eurjchem-1000	17	4	protein	protein	NOUN
eurjchem-1000	17	5	synthesis	synthesis	NOUN
eurjchem-1000	17	6	by	by	ADP
eurjchem-1000	17	7	binding	bind	VERB
eurjchem-1000	17	8	to	to	ADP
eurjchem-1000	17	9	the	the	DET
eurjchem-1000	17	10	50s	50	NOUN
eurjchem-1000	17	11	ribosomal	ribosomal	NOUN
eurjchem-1000	17	12	subunit	subunit	NOUN
eurjchem-1000	17	13	of	of	ADP
eurjchem-1000	17	14	the	the	DET
eurjchem-1000	17	15	bacterial	bacterial	ADJ
eurjchem-1000	17	16	70s	70	NOUN
eurjchem-1000	17	17	ribosome	ribosome	NOUN
eurjchem-1000	17	18	.	.	PUNCT
eurjchem-1000	18	1	it	it	PRON
eurjchem-1000	18	2	inhibits	inhibit	VERB
eurjchem-1000	18	3	peptidyl	peptidyl	NOUN
eurjchem-1000	18	4	transferase	transferase	NOUN
eurjchem-1000	18	5	activity	activity	NOUN
eurjchem-1000	18	6	and	and	CCONJ
eurjchem-1000	18	7	interferes	interfere	VERB
eurjchem-1000	18	8	with	with	ADP
eurjchem-1000	18	9	amino	amino	NOUN
eurjchem-1000	18	10	acid	acid	NOUN
eurjchem-1000	18	11	translocation	translocation	NOUN
eurjchem-1000	18	12	during	during	ADP
eurjchem-1000	18	13	the	the	DET
eurjchem-1000	18	14	process	process	NOUN
eurjchem-1000	18	15	of	of	ADP
eurjchem-1000	18	16	translation	translation	NOUN
eurjchem-1000	18	17	.	.	PUNCT
eurjchem-1000	19	1	its	its	PRON
eurjchem-1000	19	2	effect	effect	NOUN
eurjchem-1000	19	3	may	may	AUX
eurjchem-1000	19	4	be	be	AUX
eurjchem-1000	19	5	bacteriostatic	bacteriostatic	ADJ
eurjchem-1000	19	6	or	or	CCONJ
eurjchem-1000	19	7	bactericidal	bactericidal	NOUN
eurjchem-1000	19	8	depending	depend	VERB
eurjchem-1000	19	9	on	on	ADP
eurjchem-1000	19	10	the	the	DET
eurjchem-1000	19	11	organism	organism	NOUN
eurjchem-1000	19	12	and	and	CCONJ
eurjchem-1000	19	13	the	the	DET
eurjchem-1000	19	14	drug	drug	NOUN
eurjchem-1000	19	15	concentration	concentration	NOUN
eurjchem-1000	19	16	.	.	PUNCT
eurjchem-1000	20	1	its	its	PRON
eurjchem-1000	20	2	long	long	ADJ
eurjchem-1000	20	3	half‐life	half‐life	NOUN
eurjchem-1000	20	4	,	,	PUNCT
eurjchem-1000	20	5	which	which	PRON
eurjchem-1000	20	6	enables	enable	VERB
eurjchem-1000	20	7	once	once	ADV
eurjchem-1000	20	8	daily	daily	ADV
eurjchem-1000	20	9	dosing	dose	VERB
eurjchem-1000	20	10	and	and	CCONJ
eurjchem-1000	20	11	shorter	short	ADJ
eurjchem-1000	20	12	administration	administration	NOUN
eurjchem-1000	20	13	durations	duration	NOUN
eurjchem-1000	20	14	,	,	PUNCT
eurjchem-1000	20	15	is	be	AUX
eurjchem-1000	20	16	a	a	DET
eurjchem-1000	20	17	property	property	NOUN
eurjchem-1000	20	18	distinct	distinct	NOUN
eurjchem-1000	20	19	from	from	ADP
eurjchem-1000	20	20	other	other	ADJ
eurjchem-1000	20	21	macrolides	macrolide	NOUN
eurjchem-1000	20	22	.	.	PUNCT
eurjchem-1000	21	1	it	it	PRON
eurjchem-1000	21	2	is	be	AUX
eurjchem-1000	21	3	derived	derive	VERB
eurjchem-1000	21	4	from	from	ADP
eurjchem-1000	21	5	erythromycin	erythromycin	NOUN
eurjchem-1000	21	6	;	;	PUNCT
eurjchem-1000	21	7	however	however	ADV
eurjchem-1000	21	8	,	,	PUNCT
eurjchem-1000	21	9	it	it	PRON
eurjchem-1000	21	10	differs	differ	VERB
eurjchem-1000	21	11	chemically	chemically	ADV
eurjchem-1000	21	12	from	from	ADP
eurjchem-1000	21	13	erythromycin	erythromycin	NOUN
eurjchem-1000	21	14	in	in	ADP
eurjchem-1000	21	15	that	that	PRON
eurjchem-1000	21	16	a	a	DET
eurjchem-1000	21	17	methyl‐substituted	methyl‐substituted	ADJ
eurjchem-1000	21	18	nitrogen	nitrogen	NOUN
eurjchem-1000	21	19	atom	atom	NOUN
eurjchem-1000	21	20	is	be	AUX
eurjchem-1000	21	21	incorporated	incorporate	VERB
eurjchem-1000	21	22	into	into	ADP
eurjchem-1000	21	23	the	the	DET
eurjchem-1000	21	24	lactone	lactone	NOUN
eurjchem-1000	21	25	ring	ring	NOUN
eurjchem-1000	21	26	as	as	SCONJ
eurjchem-1000	21	27	shown	show	VERB
eurjchem-1000	21	28	in	in	ADP
eurjchem-1000	21	29	figure	figure	NOUN
eurjchem-1000	21	30	1	1	NUM
eurjchem-1000	21	31	.	.	PUNCT
eurjchem-1000	22	1	like	like	ADP
eurjchem-1000	22	2	erythromycin	erythromycin	PROPN
eurjchem-1000	22	3	,	,	PUNCT
eurjchem-1000	22	4	it	it	PRON
eurjchem-1000	22	5	appears	appear	VERB
eurjchem-1000	22	6	to	to	PART
eurjchem-1000	22	7	bind	bind	VERB
eurjchem-1000	22	8	to	to	ADP
eurjchem-1000	22	9	the	the	DET
eurjchem-1000	22	10	same	same	ADJ
eurjchem-1000	22	11	receptor	receptor	NOUN
eurjchem-1000	22	12	,	,	PUNCT
eurjchem-1000	22	13	50s	50	NOUN
eurjchem-1000	22	14	ribosomal	ribosomal	NOUN
eurjchem-1000	22	15	subunits	subunit	NOUN
eurjchem-1000	22	16	of	of	ADP
eurjchem-1000	22	17	susceptible	susceptible	ADJ
eurjchem-1000	22	18	bacteria	bacteria	NOUN
eurjchem-1000	22	19	and	and	CCONJ
eurjchem-1000	22	20	suppresses	suppress	VERB
eurjchem-1000	22	21	protein	protein	NOUN
eurjchem-1000	22	22	synthesis	synthesis	NOUN
eurjchem-1000	22	23	.	.	PUNCT
eurjchem-1000	23	1	it	it	PRON
eurjchem-1000	23	2	is	be	AUX
eurjchem-1000	23	3	used	use	VERB
eurjchem-1000	23	4	primarily	primarily	ADV
eurjchem-1000	23	5	to	to	PART
eurjchem-1000	23	6	treat	treat	VERB
eurjchem-1000	23	7	various	various	ADJ
eurjchem-1000	23	8	bacterial	bacterial	ADJ
eurjchem-1000	23	9	infections	infection	NOUN
eurjchem-1000	23	10	,	,	PUNCT
eurjchem-1000	23	11	such	such	ADJ
eurjchem-1000	23	12	as	as	ADP
eurjchem-1000	23	13	aerobic	aerobic	ADJ
eurjchem-1000	23	14	gram‐positive	gram‐positive	ADJ
eurjchem-1000	23	15	microorganisms	microorganism	NOUN
eurjchem-1000	23	16	and	and	CCONJ
eurjchem-1000	23	17	aerobic	aerobic	ADJ
eurjchem-1000	23	18	gram‐negative	gram‐negative	ADJ
eurjchem-1000	23	19	microorganisms	microorganism	NOUN
eurjchem-1000	23	20	.	.	PUNCT
eurjchem-1000	24	1	the	the	DET
eurjchem-1000	24	2	incorporation	incorporation	NOUN
eurjchem-1000	24	3	of	of	ADP
eurjchem-1000	24	4	the	the	DET
eurjchem-1000	24	5	nitrogen	nitrogen	NOUN
eurjchem-1000	24	6	into	into	ADP
eurjchem-1000	24	7	the	the	DET
eurjchem-1000	24	8	ring	ring	NOUN
eurjchem-1000	24	9	significantly	significantly	ADV
eurjchem-1000	24	10	alters	alter	VERB
eurjchem-1000	24	11	the	the	DET
eurjchem-1000	24	12	chemical	chemical	NOUN
eurjchem-1000	24	13	,	,	PUNCT
eurjchem-1000	24	14	microbiologic	microbiologic	ADJ
eurjchem-1000	24	15	and	and	CCONJ
eurjchem-1000	24	16	pharmacokinetic	pharmacokinetic	ADJ
eurjchem-1000	24	17	properties	property	NOUN
eurjchem-1000	24	18	of	of	ADP
eurjchem-1000	24	19	azi	azi	NOUN
eurjchem-1000	24	20	.	.	PUNCT
eurjchem-1000	25	1	it	it	PRON
eurjchem-1000	25	2	exhibits	exhibit	VERB
eurjchem-1000	25	3	a	a	DET
eurjchem-1000	25	4	more	more	ADV
eurjchem-1000	25	5	extensive	extensive	ADJ
eurjchem-1000	25	6	spectrum	spectrum	NOUN
eurjchem-1000	25	7	of	of	ADP
eurjchem-1000	25	8	activity	activity	NOUN
eurjchem-1000	25	9	,	,	PUNCT
eurjchem-1000	25	10	greater	great	ADJ
eurjchem-1000	25	11	acid	acid	NOUN
eurjchem-1000	25	12	stability	stability	NOUN
eurjchem-1000	25	13	and	and	CCONJ
eurjchem-1000	25	14	more	more	ADV
eurjchem-1000	25	15	favorable	favorable	ADJ
eurjchem-1000	25	16	pharmacokinetic	pharmacokinetic	ADJ
eurjchem-1000	25	17	parameters	parameter	NOUN
eurjchem-1000	25	18	than	than	ADP
eurjchem-1000	25	19	erythromycin	erythromycin	NOUN
eurjchem-1000	25	20	[	[	X
eurjchem-1000	25	21	1	1	NUM
eurjchem-1000	25	22	]	]	PUNCT
eurjchem-1000	25	23	.	.	PUNCT
eurjchem-1000	26	1	figure	figure	NOUN
eurjchem-1000	26	2	1	1	NUM
eurjchem-1000	26	3	.	.	PUNCT
eurjchem-1000	26	4	chemical	chemical	ADJ
eurjchem-1000	26	5	structure	structure	NOUN
eurjchem-1000	26	6	of	of	ADP
eurjchem-1000	26	7	azithromycin	azithromycin	PROPN
eurjchem-1000	26	8	.	.	PUNCT
eurjchem-1000	27	1	several	several	ADJ
eurjchem-1000	27	2	methods	method	NOUN
eurjchem-1000	27	3	have	have	AUX
eurjchem-1000	27	4	been	be	AUX
eurjchem-1000	27	5	developed	develop	VERB
eurjchem-1000	27	6	for	for	ADP
eurjchem-1000	27	7	determination	determination	NOUN
eurjchem-1000	27	8	of	of	ADP
eurjchem-1000	27	9	azi	azi	NOUN
eurjchem-1000	27	10	in	in	ADP
eurjchem-1000	27	11	pharmaceutical	pharmaceutical	ADJ
eurjchem-1000	27	12	dosage	dosage	NOUN
eurjchem-1000	27	13	forms	form	NOUN
eurjchem-1000	27	14	.	.	PUNCT
eurjchem-1000	28	1	these	these	DET
eurjchem-1000	28	2	methods	method	NOUN
eurjchem-1000	28	3	include	include	VERB
eurjchem-1000	28	4	242	242	NUM
eurjchem-1000	28	5	younes	youne	NOUN
eurjchem-1000	28	6	and	and	CCONJ
eurjchem-1000	28	7	el‐kady	el‐kady	PROPN
eurjchem-1000	28	8	/	/	SYM
eurjchem-1000	28	9	european	european	PROPN
eurjchem-1000	28	10	journal	journal	PROPN
eurjchem-1000	28	11	of	of	ADP
eurjchem-1000	28	12	chemistry	chemistry	NOUN
eurjchem-1000	28	13	5	5	NUM
eurjchem-1000	28	14	(	(	PUNCT
eurjchem-1000	28	15	2	2	NUM
eurjchem-1000	28	16	)	)	PUNCT
eurjchem-1000	28	17	(	(	PUNCT
eurjchem-1000	28	18	2014	2014	NUM
eurjchem-1000	28	19	)	)	PUNCT
eurjchem-1000	28	20	241‐246	241‐246	NUM
eurjchem-1000	28	21	high‐performance	high‐performance	PROPN
eurjchem-1000	28	22	liquid	liquid	ADJ
eurjchem-1000	28	23	chromatography	chromatography	NOUN
eurjchem-1000	28	24	(	(	PUNCT
eurjchem-1000	28	25	hplc	hplc	PROPN
eurjchem-1000	28	26	)	)	PUNCT
eurjchem-1000	28	27	and	and	CCONJ
eurjchem-1000	28	28	micro‐	micro‐	NUM
eurjchem-1000	28	29	biological	biological	ADJ
eurjchem-1000	28	30	methods	method	NOUN
eurjchem-1000	28	31	.	.	PUNCT
eurjchem-1000	29	1	chromatographic	chromatographic	ADJ
eurjchem-1000	29	2	separation	separation	NOUN
eurjchem-1000	29	3	is	be	AUX
eurjchem-1000	29	4	one	one	NUM
eurjchem-1000	29	5	of	of	ADP
eurjchem-1000	29	6	the	the	DET
eurjchem-1000	29	7	essential	essential	ADJ
eurjchem-1000	29	8	and	and	CCONJ
eurjchem-1000	29	9	powerful	powerful	ADJ
eurjchem-1000	29	10	components	component	NOUN
eurjchem-1000	29	11	of	of	ADP
eurjchem-1000	29	12	the	the	DET
eurjchem-1000	29	13	most	most	ADV
eurjchem-1000	29	14	quantitative	quantitative	ADJ
eurjchem-1000	29	15	analyses	analysis	NOUN
eurjchem-1000	29	16	and	and	CCONJ
eurjchem-1000	29	17	hplc	hplc	NOUN
eurjchem-1000	29	18	is	be	AUX
eurjchem-1000	29	19	currently	currently	ADV
eurjchem-1000	29	20	the	the	DET
eurjchem-1000	29	21	most	most	ADV
eurjchem-1000	29	22	versatile	versatile	ADJ
eurjchem-1000	29	23	tool	tool	NOUN
eurjchem-1000	29	24	which	which	PRON
eurjchem-1000	29	25	satisfies	satisfy	VERB
eurjchem-1000	29	26	the	the	DET
eurjchem-1000	29	27	needs	need	NOUN
eurjchem-1000	29	28	for	for	ADP
eurjchem-1000	29	29	an	an	DET
eurjchem-1000	29	30	optimum	optimum	ADJ
eurjchem-1000	29	31	separation	separation	NOUN
eurjchem-1000	30	1	[	[	X
eurjchem-1000	30	2	2	2	NUM
eurjchem-1000	30	3	]	]	PUNCT
eurjchem-1000	30	4	.	.	PUNCT
eurjchem-1000	31	1	azi	azi	PROPN
eurjchem-1000	31	2	has	have	AUX
eurjchem-1000	31	3	been	be	AUX
eurjchem-1000	31	4	analyzed	analyze	VERB
eurjchem-1000	31	5	by	by	ADP
eurjchem-1000	31	6	spectrophotometric	spectrophotometric	ADJ
eurjchem-1000	31	7	methods	method	NOUN
eurjchem-1000	31	8	[	[	X
eurjchem-1000	31	9	3‐5	3‐5	NUM
eurjchem-1000	31	10	]	]	PUNCT
eurjchem-1000	31	11	,	,	PUNCT
eurjchem-1000	31	12	high‐perfor‐mance	high‐perfor‐mance	NOUN
eurjchem-1000	31	13	liquid	liquid	ADJ
eurjchem-1000	31	14	chromatography	chromatography	NOUN
eurjchem-1000	31	15	using	use	VERB
eurjchem-1000	31	16	fluorescence	fluorescence	NOUN
eurjchem-1000	31	17	[	[	X
eurjchem-1000	31	18	6‐8	6‐8	NOUN
eurjchem-1000	31	19	]	]	PUNCT
eurjchem-1000	31	20	,	,	PUNCT
eurjchem-1000	31	21	electro‐chemical	electro‐chemical	ADJ
eurjchem-1000	31	22	using	use	VERB
eurjchem-1000	31	23	amperometric	amperometric	NOUN
eurjchem-1000	31	24	detection	detection	NOUN
eurjchem-1000	32	1	[	[	X
eurjchem-1000	32	2	9‐10	9‐10	X
eurjchem-1000	32	3	]	]	PUNCT
eurjchem-1000	32	4	and	and	CCONJ
eurjchem-1000	32	5	coulometric	coulometric	ADJ
eurjchem-1000	32	6	detection	detection	NOUN
eurjchem-1000	32	7	[	[	X
eurjchem-1000	32	8	11‐13	11‐13	NUM
eurjchem-1000	32	9	]	]	PUNCT
eurjchem-1000	32	10	and	and	CCONJ
eurjchem-1000	32	11	mass	mass	ADJ
eurjchem-1000	32	12	spectrometry	spectrometry	NOUN
eurjchem-1000	32	13	detector	detector	NOUN
eurjchem-1000	32	14	[	[	X
eurjchem-1000	32	15	14‐17	14‐17	X
eurjchem-1000	32	16	]	]	X
eurjchem-1000	32	17	for	for	ADP
eurjchem-1000	32	18	quantification	quantification	NOUN
eurjchem-1000	32	19	in	in	ADP
eurjchem-1000	32	20	bulk	bulk	ADJ
eurjchem-1000	32	21	material	material	NOUN
eurjchem-1000	32	22	and	and	CCONJ
eurjchem-1000	32	23	pharmaceutical	pharmaceutical	ADJ
eurjchem-1000	32	24	dosage	dosage	NOUN
eurjchem-1000	32	25	forms	form	NOUN
eurjchem-1000	32	26	.	.	PUNCT
eurjchem-1000	33	1	fluorescence	fluorescence	NOUN
eurjchem-1000	33	2	detection	detection	NOUN
eurjchem-1000	33	3	requires	require	VERB
eurjchem-1000	33	4	complicated	complicated	ADJ
eurjchem-1000	33	5	sample	sample	NOUN
eurjchem-1000	33	6	pretreatment	pretreatment	NOUN
eurjchem-1000	33	7	involving	involve	VERB
eurjchem-1000	33	8	pre‐column	pre‐column	NOUN
eurjchem-1000	33	9	derivatization	derivatization	NOUN
eurjchem-1000	33	10	of	of	ADP
eurjchem-1000	33	11	the	the	DET
eurjchem-1000	33	12	analyte	analyte	NOUN
eurjchem-1000	33	13	.	.	PUNCT
eurjchem-1000	34	1	assay	assay	NOUN
eurjchem-1000	34	2	procedures	procedure	NOUN
eurjchem-1000	34	3	making	make	VERB
eurjchem-1000	34	4	use	use	NOUN
eurjchem-1000	34	5	of	of	ADP
eurjchem-1000	34	6	electrochemical	electrochemical	ADJ
eurjchem-1000	34	7	detection	detection	NOUN
eurjchem-1000	34	8	is	be	AUX
eurjchem-1000	34	9	often	often	ADV
eurjchem-1000	34	10	very	very	ADV
eurjchem-1000	34	11	time	time	NOUN
eurjchem-1000	34	12	consuming	consume	VERB
eurjchem-1000	34	13	,	,	PUNCT
eurjchem-1000	34	14	both	both	CCONJ
eurjchem-1000	34	15	in	in	ADP
eurjchem-1000	34	16	the	the	DET
eurjchem-1000	34	17	sample	sample	NOUN
eurjchem-1000	34	18	preparation	preparation	NOUN
eurjchem-1000	34	19	steps	step	NOUN
eurjchem-1000	34	20	and	and	CCONJ
eurjchem-1000	34	21	the	the	DET
eurjchem-1000	34	22	chromatography	chromatography	NOUN
eurjchem-1000	34	23	.	.	PUNCT
eurjchem-1000	35	1	the	the	DET
eurjchem-1000	35	2	united	united	PROPN
eurjchem-1000	35	3	states	states	PROPN
eurjchem-1000	35	4	pharmacopoeaia	pharmacopoeaia	PROPN
eurjchem-1000	35	5	(	(	PUNCT
eurjchem-1000	35	6	usp	usp	NOUN
eurjchem-1000	35	7	)	)	PUNCT
eurjchem-1000	35	8	method	method	NOUN
eurjchem-1000	35	9	[	[	X
eurjchem-1000	35	10	18	18	NUM
eurjchem-1000	35	11	]	]	PUNCT
eurjchem-1000	35	12	describes	describe	VERB
eurjchem-1000	35	13	a	a	DET
eurjchem-1000	35	14	high	high	ADJ
eurjchem-1000	35	15	ph	ph	ADJ
eurjchem-1000	35	16	mobile	mobile	NOUN
eurjchem-1000	35	17	phase	phase	NOUN
eurjchem-1000	35	18	(	(	PUNCT
eurjchem-1000	35	19	ph	ph	NOUN
eurjchem-1000	35	20	=	=	NOUN
eurjchem-1000	35	21	11	11	NUM
eurjchem-1000	35	22	)	)	PUNCT
eurjchem-1000	35	23	as	as	ADV
eurjchem-1000	35	24	well	well	ADV
eurjchem-1000	35	25	as	as	ADP
eurjchem-1000	35	26	a	a	DET
eurjchem-1000	35	27	specific	specific	ADJ
eurjchem-1000	35	28	column	column	NOUN
eurjchem-1000	35	29	(	(	PUNCT
eurjchem-1000	35	30	gamma	gamma	PROPN
eurjchem-1000	35	31	alumina	alumina	PROPN
eurjchem-1000	35	32	)	)	PUNCT
eurjchem-1000	35	33	which	which	PRON
eurjchem-1000	35	34	is	be	AUX
eurjchem-1000	35	35	quite	quite	ADV
eurjchem-1000	35	36	expensive	expensive	ADJ
eurjchem-1000	35	37	and	and	CCONJ
eurjchem-1000	35	38	difficult	difficult	ADJ
eurjchem-1000	35	39	to	to	PART
eurjchem-1000	35	40	obtain	obtain	VERB
eurjchem-1000	35	41	commercially	commercially	ADV
eurjchem-1000	35	42	as	as	ADP
eurjchem-1000	35	43	many	many	ADJ
eurjchem-1000	35	44	of	of	ADP
eurjchem-1000	35	45	the	the	DET
eurjchem-1000	35	46	column	column	NOUN
eurjchem-1000	35	47	manufacturers	manufacturer	NOUN
eurjchem-1000	35	48	do	do	AUX
eurjchem-1000	35	49	not	not	PART
eurjchem-1000	35	50	supply	supply	VERB
eurjchem-1000	35	51	this	this	DET
eurjchem-1000	35	52	column	column	NOUN
eurjchem-1000	35	53	.	.	PUNCT
eurjchem-1000	36	1	also	also	ADV
eurjchem-1000	36	2	,	,	PUNCT
eurjchem-1000	36	3	the	the	DET
eurjchem-1000	36	4	usp	usp	NOUN
eurjchem-1000	36	5	method	method	NOUN
eurjchem-1000	36	6	employs	employ	VERB
eurjchem-1000	36	7	amperometric	amperometric	NOUN
eurjchem-1000	36	8	electrochemical	electrochemical	ADJ
eurjchem-1000	36	9	detection	detection	NOUN
eurjchem-1000	36	10	,	,	PUNCT
eurjchem-1000	36	11	which	which	PRON
eurjchem-1000	36	12	is	be	AUX
eurjchem-1000	36	13	not	not	PART
eurjchem-1000	36	14	available	available	ADJ
eurjchem-1000	36	15	in	in	ADP
eurjchem-1000	36	16	many	many	ADJ
eurjchem-1000	36	17	laboratories	laboratory	NOUN
eurjchem-1000	36	18	.	.	PUNCT
eurjchem-1000	37	1	therefore	therefore	ADV
eurjchem-1000	37	2	,	,	PUNCT
eurjchem-1000	37	3	there	there	PRON
eurjchem-1000	37	4	is	be	VERB
eurjchem-1000	37	5	a	a	DET
eurjchem-1000	37	6	need	need	NOUN
eurjchem-1000	37	7	for	for	ADP
eurjchem-1000	37	8	a	a	DET
eurjchem-1000	37	9	convenient	convenient	ADJ
eurjchem-1000	37	10	and	and	CCONJ
eurjchem-1000	37	11	effective	effective	ADJ
eurjchem-1000	37	12	method	method	NOUN
eurjchem-1000	37	13	for	for	ADP
eurjchem-1000	37	14	determination	determination	NOUN
eurjchem-1000	37	15	of	of	ADP
eurjchem-1000	37	16	azi	azi	NOUN
eurjchem-1000	37	17	in	in	ADP
eurjchem-1000	37	18	pharmaceutical	pharmaceutical	ADJ
eurjchem-1000	37	19	dosage	dosage	NOUN
eurjchem-1000	37	20	forms	form	NOUN
eurjchem-1000	37	21	.	.	PUNCT
eurjchem-1000	38	1	liquid	liquid	ADJ
eurjchem-1000	38	2	chromatography	chromatography	NOUN
eurjchem-1000	38	3	with	with	ADP
eurjchem-1000	38	4	uv	uv	NOUN
eurjchem-1000	38	5	detection	detection	NOUN
eurjchem-1000	38	6	has	have	AUX
eurjchem-1000	38	7	been	be	AUX
eurjchem-1000	38	8	already	already	ADV
eurjchem-1000	38	9	employed	employ	VERB
eurjchem-1000	38	10	for	for	ADP
eurjchem-1000	38	11	the	the	DET
eurjchem-1000	38	12	analysis	analysis	NOUN
eurjchem-1000	38	13	of	of	ADP
eurjchem-1000	38	14	azi	azi	NOUN
eurjchem-1000	38	15	either	either	CCONJ
eurjchem-1000	38	16	in	in	ADP
eurjchem-1000	38	17	tablets	tablet	NOUN
eurjchem-1000	38	18	[	[	X
eurjchem-1000	38	19	19	19	NUM
eurjchem-1000	38	20	]	]	PUNCT
eurjchem-1000	38	21	or	or	CCONJ
eurjchem-1000	38	22	in	in	ADP
eurjchem-1000	38	23	raw	raw	ADJ
eurjchem-1000	38	24	material	material	NOUN
eurjchem-1000	38	25	[	[	X
eurjchem-1000	38	26	20	20	NUM
eurjchem-1000	38	27	]	]	PUNCT
eurjchem-1000	38	28	or	or	CCONJ
eurjchem-1000	38	29	in	in	ADP
eurjchem-1000	38	30	both	both	PRON
eurjchem-1000	38	31	[	[	X
eurjchem-1000	38	32	21	21	NUM
eurjchem-1000	38	33	]	]	PUNCT
eurjchem-1000	38	34	.	.	PUNCT
eurjchem-1000	39	1	mass	mass	PROPN
eurjchem-1000	39	2	spectrometry	spectrometry	NOUN
eurjchem-1000	39	3	methods	method	NOUN
eurjchem-1000	39	4	may	may	AUX
eurjchem-1000	39	5	have	have	VERB
eurjchem-1000	39	6	the	the	DET
eurjchem-1000	39	7	highest	high	ADJ
eurjchem-1000	39	8	sensitivity	sensitivity	NOUN
eurjchem-1000	39	9	,	,	PUNCT
eurjchem-1000	39	10	but	but	CCONJ
eurjchem-1000	39	11	the	the	DET
eurjchem-1000	39	12	determination	determination	NOUN
eurjchem-1000	39	13	process	process	NOUN
eurjchem-1000	39	14	is	be	AUX
eurjchem-1000	39	15	complex	complex	ADJ
eurjchem-1000	40	1	[	[	X
eurjchem-1000	40	2	22	22	NUM
eurjchem-1000	40	3	]	]	PUNCT
eurjchem-1000	40	4	.	.	PUNCT
eurjchem-1000	41	1	various	various	ADJ
eurjchem-1000	41	2	extraction	extraction	NOUN
eurjchem-1000	41	3	methods	method	NOUN
eurjchem-1000	41	4	have	have	AUX
eurjchem-1000	41	5	been	be	AUX
eurjchem-1000	41	6	reported	report	VERB
eurjchem-1000	41	7	for	for	ADP
eurjchem-1000	41	8	extraction	extraction	NOUN
eurjchem-1000	41	9	of	of	ADP
eurjchem-1000	41	10	azithromycin	azithromycin	NOUN
eurjchem-1000	41	11	form	form	NOUN
eurjchem-1000	41	12	plasma	plasma	NOUN
eurjchem-1000	41	13	like	like	ADP
eurjchem-1000	41	14	,	,	PUNCT
eurjchem-1000	41	15	protein	protein	NOUN
eurjchem-1000	41	16	precipitation	precipitation	NOUN
eurjchem-1000	42	1	[	[	X
eurjchem-1000	42	2	23,24	23,24	ADP
eurjchem-1000	42	3	]	]	PUNCT
eurjchem-1000	42	4	,	,	PUNCT
eurjchem-1000	42	5	pressurized	pressurize	VERB
eurjchem-1000	42	6	liquid	liquid	ADJ
eurjchem-1000	42	7	extraction	extraction	NOUN
eurjchem-1000	42	8	(	(	PUNCT
eurjchem-1000	42	9	ple	ple	NOUN
eurjchem-1000	42	10	)	)	PUNCT
eurjchem-1000	43	1	[	[	X
eurjchem-1000	43	2	25	25	NUM
eurjchem-1000	43	3	]	]	PUNCT
eurjchem-1000	43	4	,	,	PUNCT
eurjchem-1000	43	5	liquid‐liquid	liquid‐liquid	ADJ
eurjchem-1000	43	6	extraction	extraction	NOUN
eurjchem-1000	43	7	[	[	X
eurjchem-1000	43	8	26,27	26,27	NUM
eurjchem-1000	43	9	]	]	PUNCT
eurjchem-1000	43	10	and	and	CCONJ
eurjchem-1000	43	11	solid	solid	ADJ
eurjchem-1000	43	12	phase	phase	NOUN
eurjchem-1000	43	13	extraction	extraction	NOUN
eurjchem-1000	43	14	[	[	X
eurjchem-1000	43	15	28,29	28,29	NUM
eurjchem-1000	43	16	]	]	X
eurjchem-1000	43	17	.	.	PUNCT
eurjchem-1000	44	1	the	the	DET
eurjchem-1000	44	2	objective	objective	NOUN
eurjchem-1000	44	3	of	of	ADP
eurjchem-1000	44	4	the	the	DET
eurjchem-1000	44	5	study	study	NOUN
eurjchem-1000	44	6	was	be	AUX
eurjchem-1000	44	7	to	to	PART
eurjchem-1000	44	8	develop	develop	VERB
eurjchem-1000	44	9	simple	simple	ADJ
eurjchem-1000	44	10	,	,	PUNCT
eurjchem-1000	44	11	fast	fast	ADJ
eurjchem-1000	44	12	,	,	PUNCT
eurjchem-1000	44	13	sensitive	sensitive	ADJ
eurjchem-1000	44	14	,	,	PUNCT
eurjchem-1000	44	15	selective	selective	ADJ
eurjchem-1000	44	16	,	,	PUNCT
eurjchem-1000	44	17	accurate	accurate	ADJ
eurjchem-1000	44	18	and	and	CCONJ
eurjchem-1000	44	19	economic	economic	ADJ
eurjchem-1000	44	20	method	method	NOUN
eurjchem-1000	44	21	for	for	ADP
eurjchem-1000	44	22	quantification	quantification	NOUN
eurjchem-1000	44	23	of	of	ADP
eurjchem-1000	44	24	azithromycin	azithromycin	PROPN
eurjchem-1000	44	25	in	in	ADP
eurjchem-1000	44	26	human	human	ADJ
eurjchem-1000	44	27	plasma	plasma	NOUN
eurjchem-1000	44	28	following	follow	VERB
eurjchem-1000	44	29	liquid‐liquid	liquid‐liquid	NOUN
eurjchem-1000	44	30	extraction	extraction	NOUN
eurjchem-1000	44	31	by	by	ADP
eurjchem-1000	44	32	lc‐ms	lc‐ms	SYM
eurjchem-1000	44	33	/	/	SYM
eurjchem-1000	44	34	ms	ms	PROPN
eurjchem-1000	44	35	.	.	PROPN
eurjchem-1000	45	1	unlike	unlike	ADP
eurjchem-1000	45	2	other	other	ADJ
eurjchem-1000	45	3	lc‐ms	lc‐ms	PROPN
eurjchem-1000	45	4	methods	method	NOUN
eurjchem-1000	45	5	,	,	PUNCT
eurjchem-1000	45	6	the	the	DET
eurjchem-1000	45	7	presented	present	VERB
eurjchem-1000	45	8	method	method	NOUN
eurjchem-1000	45	9	has	have	VERB
eurjchem-1000	45	10	the	the	DET
eurjchem-1000	45	11	advantages	advantage	NOUN
eurjchem-1000	45	12	of	of	ADP
eurjchem-1000	45	13	short	short	ADJ
eurjchem-1000	45	14	run	run	NOUN
eurjchem-1000	45	15	time	time	NOUN
eurjchem-1000	45	16	(	(	PUNCT
eurjchem-1000	45	17	about	about	ADP
eurjchem-1000	45	18	0.5	0.5	NUM
eurjchem-1000	45	19	min	min	NOUN
eurjchem-1000	45	20	)	)	PUNCT
eurjchem-1000	45	21	which	which	PRON
eurjchem-1000	45	22	made	make	VERB
eurjchem-1000	45	23	it	it	PRON
eurjchem-1000	45	24	possible	possible	ADJ
eurjchem-1000	45	25	to	to	PART
eurjchem-1000	45	26	analyze	analyze	VERB
eurjchem-1000	45	27	more	more	ADJ
eurjchem-1000	45	28	than	than	ADP
eurjchem-1000	45	29	400	400	NUM
eurjchem-1000	45	30	plasma	plasma	NOUN
eurjchem-1000	45	31	samples	sample	NOUN
eurjchem-1000	45	32	per	per	ADP
eurjchem-1000	45	33	day	day	NOUN
eurjchem-1000	45	34	and	and	CCONJ
eurjchem-1000	45	35	a	a	DET
eurjchem-1000	45	36	wide	wide	ADJ
eurjchem-1000	45	37	range	range	NOUN
eurjchem-1000	45	38	of	of	ADP
eurjchem-1000	45	39	linearity	linearity	NOUN
eurjchem-1000	45	40	(	(	PUNCT
eurjchem-1000	45	41	5‐1500	5‐1500	NUM
eurjchem-1000	45	42	ng	ng	PROPN
eurjchem-1000	45	43	/	/	SYM
eurjchem-1000	45	44	ml	ml	NOUN
eurjchem-1000	45	45	)	)	PUNCT
eurjchem-1000	45	46	.	.	PUNCT
eurjchem-1000	46	1	sildenafil	sildenafil	PROPN
eurjchem-1000	46	2	citrate	citrate	PROPN
eurjchem-1000	46	3	(	(	PUNCT
eurjchem-1000	46	4	figure	figure	NOUN
eurjchem-1000	46	5	2	2	NUM
eurjchem-1000	46	6	)	)	PUNCT
eurjchem-1000	46	7	,	,	PUNCT
eurjchem-1000	46	8	designated	designate	VERB
eurjchem-1000	46	9	chemically	chemically	ADV
eurjchem-1000	46	10	as	as	ADP
eurjchem-1000	46	11	1‐[[3‐(6,7‐dihydro‐1‐methyl‐7‐oxo‐3‐	1‐[[3‐(6,7‐dihydro‐1‐methyl‐7‐oxo‐3‐	NUM
eurjchem-1000	46	12	propyl‐1hpyrazolo[4,3‐d]pyrimidin‐5‐yl)‐4‐ethoxyphenyl	propyl‐1hpyrazolo[4,3‐d]pyrimidin‐5‐yl)‐4‐ethoxyphenyl	NOUN
eurjchem-1000	46	13	]	]	PUNCT
eurjchem-1000	46	14	sulfonyl]‐4‐methylpiperazine	sulfonyl]‐4‐methylpiperazine	NOUN
eurjchem-1000	46	15	citrate	citrate	NOUN
eurjchem-1000	46	16	was	be	AUX
eurjchem-1000	46	17	used	use	VERB
eurjchem-1000	46	18	as	as	ADP
eurjchem-1000	46	19	internal	internal	ADJ
eurjchem-1000	46	20	standard	standard	NOUN
eurjchem-1000	46	21	(	(	PUNCT
eurjchem-1000	46	22	is	be	AUX
eurjchem-1000	46	23	)	)	PUNCT
eurjchem-1000	46	24	.	.	PUNCT
eurjchem-1000	47	1	figure	figure	NOUN
eurjchem-1000	47	2	2	2	NUM
eurjchem-1000	47	3	.	.	PUNCT
eurjchem-1000	47	4	chemical	chemical	ADJ
eurjchem-1000	47	5	structure	structure	NOUN
eurjchem-1000	47	6	of	of	ADP
eurjchem-1000	47	7	sildenafil	sildenafil	NOUN
eurjchem-1000	47	8	citrate	citrate	NOUN
eurjchem-1000	47	9	(	(	PUNCT
eurjchem-1000	47	10	is	be	AUX
eurjchem-1000	47	11	)	)	PUNCT
eurjchem-1000	47	12	.	.	PUNCT
eurjchem-1000	48	1	2	2	X
eurjchem-1000	48	2	.	.	X
eurjchem-1000	48	3	experimental	experimental	ADJ
eurjchem-1000	48	4	2.1	2.1	NUM
eurjchem-1000	48	5	.	.	PUNCT
eurjchem-1000	48	6	chemicals	chemical	NOUN
eurjchem-1000	48	7	and	and	CCONJ
eurjchem-1000	48	8	reagents	reagent	NOUN
eurjchem-1000	48	9	azithromycin	azithromycin	PROPN
eurjchem-1000	48	10	reference	reference	NOUN
eurjchem-1000	48	11	standard	standard	NOUN
eurjchem-1000	48	12	(	(	PUNCT
eurjchem-1000	48	13	b.n	b.n	PROPN
eurjchem-1000	48	14	:	:	PUNCT
eurjchem-1000	48	15	1182090426	1182090426	NUM
eurjchem-1000	48	16	;	;	PUNCT
eurjchem-1000	48	17	purity	purity	NOUN
eurjchem-1000	48	18	:	:	PUNCT
eurjchem-1000	48	19	97.80	97.80	NUM
eurjchem-1000	48	20	%	%	NOUN
eurjchem-1000	48	21	)	)	PUNCT
eurjchem-1000	48	22	was	be	AUX
eurjchem-1000	48	23	obtained	obtain	VERB
eurjchem-1000	48	24	from	from	ADP
eurjchem-1000	48	25	cspc	cspc	NOUN
eurjchem-1000	48	26	,	,	PUNCT
eurjchem-1000	48	27	ouyi	ouyi	PROPN
eurjchem-1000	48	28	pharmaceutical	pharmaceutical	PROPN
eurjchem-1000	48	29	co.	co.	PROPN
eurjchem-1000	48	30	ltd	ltd	PROPN
eurjchem-1000	48	31	(	(	PUNCT
eurjchem-1000	48	32	shijiazhuang	shijiazhuang	PROPN
eurjchem-1000	48	33	,	,	PUNCT
eurjchem-1000	48	34	china	china	PROPN
eurjchem-1000	48	35	)	)	PUNCT
eurjchem-1000	48	36	.	.	PUNCT
eurjchem-1000	49	1	sildenafil	sildenafil	PROPN
eurjchem-1000	49	2	citrate	citrate	PROPN
eurjchem-1000	49	3	(	(	PUNCT
eurjchem-1000	49	4	b.n	b.n	PROPN
eurjchem-1000	49	5	.	.	PROPN
eurjchem-1000	49	6	586032009sc	586032009sc	NOUN
eurjchem-1000	49	7	;	;	PUNCT
eurjchem-1000	49	8	purity	purity	NOUN
eurjchem-1000	49	9	:	:	PUNCT
eurjchem-1000	49	10	99.20	99.20	NUM
eurjchem-1000	49	11	%	%	NOUN
eurjchem-1000	49	12	)	)	PUNCT
eurjchem-1000	49	13	was	be	AUX
eurjchem-1000	49	14	employed	employ	VERB
eurjchem-1000	49	15	as	as	ADP
eurjchem-1000	49	16	an	an	DET
eurjchem-1000	49	17	internal	internal	ADJ
eurjchem-1000	49	18	standard	standard	NOUN
eurjchem-1000	49	19	(	(	PUNCT
eurjchem-1000	49	20	is	be	AUX
eurjchem-1000	49	21	)	)	PUNCT
eurjchem-1000	49	22	obtained	obtain	VERB
eurjchem-1000	49	23	from	from	ADP
eurjchem-1000	49	24	bdr	bdr	PROPN
eurjchem-1000	49	25	pharmaceuticals	pharmaceuticals	PROPN
eurjchem-1000	49	26	international	international	PROPN
eurjchem-1000	49	27	pvt	pvt	PROPN
eurjchem-1000	49	28	.	.	PUNCT
eurjchem-1000	50	1	it	it	PRON
eurjchem-1000	50	2	d	d	PROPN
eurjchem-1000	50	3	(	(	PUNCT
eurjchem-1000	50	4	mumbai	mumbai	PROPN
eurjchem-1000	50	5	,	,	PUNCT
eurjchem-1000	50	6	india	india	PROPN
eurjchem-1000	50	7	)	)	PUNCT
eurjchem-1000	50	8	.	.	PUNCT
eurjchem-1000	51	1	water	water	NOUN
eurjchem-1000	51	2	for	for	ADP
eurjchem-1000	51	3	hplc	hplc	NOUN
eurjchem-1000	51	4	was	be	AUX
eurjchem-1000	51	5	purchased	purchase	VERB
eurjchem-1000	51	6	from	from	ADP
eurjchem-1000	51	7	merck	merck	PROPN
eurjchem-1000	51	8	,	,	PUNCT
eurjchem-1000	51	9	germany	germany	PROPN
eurjchem-1000	51	10	.	.	PUNCT
eurjchem-1000	52	1	formic	formic	PROPN
eurjchem-1000	52	2	acid	acid	PROPN
eurjchem-1000	52	3	and	and	CCONJ
eurjchem-1000	52	4	acetonitrile	acetonitrile	NOUN
eurjchem-1000	52	5	were	be	AUX
eurjchem-1000	52	6	of	of	ADP
eurjchem-1000	52	7	hplc	hplc	NOUN
eurjchem-1000	52	8	grade	grade	NOUN
eurjchem-1000	52	9	and	and	CCONJ
eurjchem-1000	52	10	purchased	purchase	VERB
eurjchem-1000	52	11	from	from	ADP
eurjchem-1000	52	12	sigma‐aldrich	sigma‐aldrich	NOUN
eurjchem-1000	52	13	chemie	chemie	PROPN
eurjchem-1000	52	14	gmbh	gmbh	PROPN
eurjchem-1000	52	15	(	(	PUNCT
eurjchem-1000	52	16	munich	munich	PROPN
eurjchem-1000	52	17	,	,	PUNCT
eurjchem-1000	52	18	germany	germany	PROPN
eurjchem-1000	52	19	)	)	PUNCT
eurjchem-1000	52	20	.	.	PUNCT
eurjchem-1000	53	1	sodium	sodium	NOUN
eurjchem-1000	53	2	carbonate	carbonate	NOUN
eurjchem-1000	53	3	and	and	CCONJ
eurjchem-1000	53	4	tert‐butyl	tert‐butyl	ADP
eurjchem-1000	53	5	methyl	methyl	NOUN
eurjchem-1000	53	6	ether	ether	NOUN
eurjchem-1000	53	7	were	be	AUX
eurjchem-1000	53	8	supplied	supply	VERB
eurjchem-1000	53	9	by	by	ADP
eurjchem-1000	53	10	(	(	PUNCT
eurjchem-1000	53	11	romil	romil	PROPN
eurjchem-1000	53	12	ltd	ltd	PROPN
eurjchem-1000	53	13	.	.	PROPN
eurjchem-1000	53	14	,	,	PUNCT
eurjchem-1000	53	15	london	london	PROPN
eurjchem-1000	53	16	,	,	PUNCT
eurjchem-1000	53	17	uk	uk	PROPN
eurjchem-1000	53	18	)	)	PUNCT
eurjchem-1000	53	19	.	.	PUNCT
eurjchem-1000	54	1	the	the	DET
eurjchem-1000	54	2	control	control	PROPN
eurjchem-1000	54	3	human	human	PROPN
eurjchem-1000	54	4	plasma	plasma	NOUN
eurjchem-1000	54	5	sample	sample	NOUN
eurjchem-1000	54	6	was	be	AUX
eurjchem-1000	54	7	procured	procure	VERB
eurjchem-1000	54	8	from	from	ADP
eurjchem-1000	54	9	vacsera	vacsera	PROPN
eurjchem-1000	54	10	(	(	PUNCT
eurjchem-1000	54	11	cairo	cairo	PROPN
eurjchem-1000	54	12	,	,	PUNCT
eurjchem-1000	54	13	egypt	egypt	PROPN
eurjchem-1000	54	14	)	)	PUNCT
eurjchem-1000	54	15	.	.	PUNCT
eurjchem-1000	55	1	2.2	2.2	NUM
eurjchem-1000	55	2	.	.	PUNCT
eurjchem-1000	56	1	equipment	equipment	NOUN
eurjchem-1000	56	2	acquity	acquity	NOUN
eurjchem-1000	56	3	ultra‐performance	ultra‐performance	ADP
eurjchem-1000	56	4	liquid	liquid	ADJ
eurjchem-1000	56	5	chromatographic‐	chromatographic‐	PROPN
eurjchem-1000	56	6	ms	ms	PROPN
eurjchem-1000	56	7	/	/	SYM
eurjchem-1000	56	8	ms	ms	PROPN
eurjchem-1000	56	9	(	(	PUNCT
eurjchem-1000	56	10	uplc‐ms	uplc‐ms	PROPN
eurjchem-1000	56	11	/	/	SYM
eurjchem-1000	56	12	ms	ms	NOUN
eurjchem-1000	56	13	)	)	PUNCT
eurjchem-1000	56	14	system	system	NOUN
eurjchem-1000	56	15	equipped	equip	VERB
eurjchem-1000	56	16	with	with	ADP
eurjchem-1000	56	17	uplc	uplc	ADJ
eurjchem-1000	56	18	c18	c18	PROPN
eurjchem-1000	56	19	(	(	PUNCT
eurjchem-1000	56	20	50	50	NUM
eurjchem-1000	56	21	×	×	NOUN
eurjchem-1000	56	22	2.1	2.1	NUM
eurjchem-1000	56	23	,	,	PUNCT
eurjchem-1000	56	24	5	5	NUM
eurjchem-1000	56	25	µm	µm	NOUN
eurjchem-1000	56	26	)	)	PUNCT
eurjchem-1000	56	27	column	column	NOUN
eurjchem-1000	56	28	,	,	PUNCT
eurjchem-1000	56	29	tandem	tandem	NOUN
eurjchem-1000	56	30	mass	mass	ADJ
eurjchem-1000	56	31	triple‐quadruple	triple‐quadruple	NOUN
eurjchem-1000	56	32	detector	detector	NOUN
eurjchem-1000	56	33	and	and	CCONJ
eurjchem-1000	56	34	electro	electro	VERB
eurjchem-1000	56	35	spray	spray	NOUN
eurjchem-1000	56	36	ionization	ionization	NOUN
eurjchem-1000	56	37	(	(	PUNCT
eurjchem-1000	56	38	esi	esi	NOUN
eurjchem-1000	56	39	)	)	PUNCT
eurjchem-1000	56	40	probe	probe	NOUN
eurjchem-1000	56	41	was	be	AUX
eurjchem-1000	56	42	used	use	VERB
eurjchem-1000	56	43	for	for	ADP
eurjchem-1000	56	44	the	the	DET
eurjchem-1000	56	45	assay	assay	NOUN
eurjchem-1000	56	46	(	(	PUNCT
eurjchem-1000	56	47	waters	water	NOUN
eurjchem-1000	56	48	,	,	PUNCT
eurjchem-1000	56	49	usa	usa	PROPN
eurjchem-1000	56	50	)	)	PUNCT
eurjchem-1000	56	51	.	.	PUNCT
eurjchem-1000	57	1	the	the	DET
eurjchem-1000	57	2	system	system	NOUN
eurjchem-1000	57	3	included	include	VERB
eurjchem-1000	57	4	a	a	DET
eurjchem-1000	57	5	vacuum	vacuum	NOUN
eurjchem-1000	57	6	degasser	degasser	NOUN
eurjchem-1000	57	7	,	,	PUNCT
eurjchem-1000	57	8	a	a	DET
eurjchem-1000	57	9	quaternary	quaternary	ADJ
eurjchem-1000	57	10	pump	pump	NOUN
eurjchem-1000	57	11	,	,	PUNCT
eurjchem-1000	57	12	a	a	DET
eurjchem-1000	57	13	thermostatted	thermostatte	VERB
eurjchem-1000	57	14	auto‐sampler	auto‐sampler	NOUN
eurjchem-1000	57	15	and	and	CCONJ
eurjchem-1000	57	16	a	a	DET
eurjchem-1000	57	17	column	column	NOUN
eurjchem-1000	57	18	oven	oven	NOUN
eurjchem-1000	57	19	compartment	compartment	NOUN
eurjchem-1000	57	20	.	.	PUNCT
eurjchem-1000	58	1	data	datum	NOUN
eurjchem-1000	58	2	acquisition	acquisition	NOUN
eurjchem-1000	58	3	and	and	CCONJ
eurjchem-1000	58	4	data	datum	NOUN
eurjchem-1000	58	5	integration	integration	NOUN
eurjchem-1000	58	6	were	be	AUX
eurjchem-1000	58	7	done	do	VERB
eurjchem-1000	58	8	using	use	VERB
eurjchem-1000	58	9	empower	empower	NOUN
eurjchem-1000	58	10	™	™	ADJ
eurjchem-1000	58	11	ver.2	ver.2	PROPN
eurjchem-1000	58	12	chromatography	chromatography	NOUN
eurjchem-1000	58	13	data	datum	NOUN
eurjchem-1000	58	14	software	software	NOUN
eurjchem-1000	58	15	(	(	PUNCT
eurjchem-1000	58	16	cds	cds	NOUN
eurjchem-1000	58	17	)	)	PUNCT
eurjchem-1000	58	18	solutions	solution	NOUN
eurjchem-1000	58	19	.	.	PUNCT
eurjchem-1000	59	1	2.3	2.3	NUM
eurjchem-1000	59	2	.	.	PUNCT
eurjchem-1000	59	3	chromatographic	chromatographic	ADJ
eurjchem-1000	59	4	conditions	condition	NOUN
eurjchem-1000	59	5	separations	separation	NOUN
eurjchem-1000	59	6	were	be	AUX
eurjchem-1000	59	7	performed	perform	VERB
eurjchem-1000	59	8	on	on	ADP
eurjchem-1000	59	9	uplc	uplc	ADJ
eurjchem-1000	59	10	c18	c18	PROPN
eurjchem-1000	59	11	(	(	PUNCT
eurjchem-1000	59	12	50	50	NUM
eurjchem-1000	59	13	×	×	NOUN
eurjchem-1000	59	14	2.1	2.1	NUM
eurjchem-1000	59	15	,	,	PUNCT
eurjchem-1000	59	16	5	5	NUM
eurjchem-1000	59	17	µm	µm	NOUN
eurjchem-1000	59	18	)	)	PUNCT
eurjchem-1000	59	19	column	column	NOUN
eurjchem-1000	59	20	.	.	PUNCT
eurjchem-1000	60	1	a	a	DET
eurjchem-1000	60	2	mobile	mobile	ADJ
eurjchem-1000	60	3	phase	phase	NOUN
eurjchem-1000	60	4	consisting	consist	VERB
eurjchem-1000	60	5	of	of	ADP
eurjchem-1000	60	6	a	a	DET
eurjchem-1000	60	7	mixture	mixture	NOUN
eurjchem-1000	60	8	of	of	ADP
eurjchem-1000	60	9	acetonitrile‐	acetonitrile‐	NOUN
eurjchem-1000	60	10	0.1	0.1	NUM
eurjchem-1000	60	11	%	%	NOUN
eurjchem-1000	60	12	formic	formic	PROPN
eurjchem-1000	60	13	acid	acid	NOUN
eurjchem-1000	60	14	(	(	PUNCT
eurjchem-1000	60	15	80:20	80:20	NUM
eurjchem-1000	60	16	,	,	PUNCT
eurjchem-1000	60	17	v	v	NOUN
eurjchem-1000	60	18	:	:	SYM
eurjchem-1000	60	19	v	v	NOUN
eurjchem-1000	60	20	)	)	PUNCT
eurjchem-1000	60	21	was	be	AUX
eurjchem-1000	60	22	delivered	deliver	VERB
eurjchem-1000	60	23	at	at	ADP
eurjchem-1000	60	24	a	a	DET
eurjchem-1000	60	25	flow	flow	NOUN
eurjchem-1000	60	26	rate	rate	NOUN
eurjchem-1000	60	27	of	of	ADP
eurjchem-1000	60	28	0.5	0.5	NUM
eurjchem-1000	60	29	ml	ml	NOUN
eurjchem-1000	60	30	/	/	SYM
eurjchem-1000	60	31	min	min	NOUN
eurjchem-1000	60	32	into	into	ADP
eurjchem-1000	60	33	the	the	DET
eurjchem-1000	60	34	mass	mass	NOUN
eurjchem-1000	60	35	spectrometer	spectrometer	NOUN
eurjchem-1000	60	36	.	.	PUNCT
eurjchem-1000	61	1	aliquot	aliquot	NOUN
eurjchem-1000	61	2	of	of	ADP
eurjchem-1000	61	3	7.5	7.5	NUM
eurjchem-1000	61	4	μl	μl	ADP
eurjchem-1000	61	5	of	of	ADP
eurjchem-1000	61	6	the	the	DET
eurjchem-1000	61	7	processed	process	VERB
eurjchem-1000	61	8	samples	sample	NOUN
eurjchem-1000	61	9	were	be	AUX
eurjchem-1000	61	10	injected	inject	VERB
eurjchem-1000	61	11	into	into	ADP
eurjchem-1000	61	12	the	the	DET
eurjchem-1000	61	13	column	column	NOUN
eurjchem-1000	61	14	,	,	PUNCT
eurjchem-1000	61	15	which	which	PRON
eurjchem-1000	61	16	was	be	AUX
eurjchem-1000	61	17	kept	keep	VERB
eurjchem-1000	61	18	at	at	ADP
eurjchem-1000	61	19	30	30	NUM
eurjchem-1000	61	20	°	°	NOUN
eurjchem-1000	61	21	c	c	NOUN
eurjchem-1000	61	22	.	.	PUNCT
eurjchem-1000	62	1	quantification	quantification	NOUN
eurjchem-1000	62	2	was	be	AUX
eurjchem-1000	62	3	achieved	achieve	VERB
eurjchem-1000	62	4	with	with	ADP
eurjchem-1000	62	5	ms‐ms	ms‐ms	NUM
eurjchem-1000	62	6	detection	detection	NOUN
eurjchem-1000	62	7	in	in	ADP
eurjchem-1000	62	8	positive	positive	ADJ
eurjchem-1000	62	9	ion	ion	NOUN
eurjchem-1000	62	10	mode	mode	NOUN
eurjchem-1000	62	11	for	for	ADP
eurjchem-1000	62	12	both	both	CCONJ
eurjchem-1000	62	13	the	the	DET
eurjchem-1000	62	14	internal	internal	ADJ
eurjchem-1000	62	15	standard	standard	NOUN
eurjchem-1000	62	16	and	and	CCONJ
eurjchem-1000	62	17	azithromycin	azithromycin	NOUN
eurjchem-1000	62	18	using	use	VERB
eurjchem-1000	62	19	waters	water	NOUN
eurjchem-1000	62	20	acquity	acquity	NOUN
eurjchem-1000	62	21	tqd	tqd	NOUN
eurjchem-1000	62	22	(	(	PUNCT
eurjchem-1000	62	23	triple	triple	ADJ
eurjchem-1000	62	24	quad	quad	ADJ
eurjchem-1000	62	25	detector	detector	NOUN
eurjchem-1000	62	26	)	)	PUNCT
eurjchem-1000	62	27	ms	ms	PROPN
eurjchem-1000	62	28	/	/	SYM
eurjchem-1000	62	29	ms	ms	PROPN
eurjchem-1000	62	30	(	(	PUNCT
eurjchem-1000	62	31	foster	foster	ADJ
eurjchem-1000	62	32	city	city	NOUN
eurjchem-1000	62	33	,	,	PUNCT
eurjchem-1000	62	34	ca	ca	PROPN
eurjchem-1000	62	35	,	,	PUNCT
eurjchem-1000	62	36	usa	usa	PROPN
eurjchem-1000	62	37	)	)	PUNCT
eurjchem-1000	62	38	.	.	PUNCT
eurjchem-1000	63	1	the	the	DET
eurjchem-1000	63	2	compound	compound	NOUN
eurjchem-1000	63	3	parameters	parameter	NOUN
eurjchem-1000	63	4	viz	viz	VERB
eurjchem-1000	63	5	.	.	PUNCT
eurjchem-1000	64	1	the	the	DET
eurjchem-1000	64	2	collision	collision	NOUN
eurjchem-1000	64	3	energy	energy	NOUN
eurjchem-1000	64	4	(	(	PUNCT
eurjchem-1000	64	5	ce	ce	PROPN
eurjchem-1000	64	6	)	)	PUNCT
eurjchem-1000	64	7	and	and	CCONJ
eurjchem-1000	64	8	cone	cone	NOUN
eurjchem-1000	64	9	voltage	voltage	NOUN
eurjchem-1000	64	10	(	(	PUNCT
eurjchem-1000	64	11	cv	cv	PROPN
eurjchem-1000	64	12	)	)	PUNCT
eurjchem-1000	64	13	were	be	AUX
eurjchem-1000	64	14	38	38	NUM
eurjchem-1000	64	15	and	and	CCONJ
eurjchem-1000	64	16	40	40	NUM
eurjchem-1000	64	17	volt	volt	NOUN
eurjchem-1000	64	18	for	for	ADP
eurjchem-1000	64	19	azithromycin	azithromycin	PROPN
eurjchem-1000	64	20	and	and	CCONJ
eurjchem-1000	64	21	30	30	NUM
eurjchem-1000	64	22	and	and	CCONJ
eurjchem-1000	64	23	50	50	NUM
eurjchem-1000	64	24	volt	volt	NOUN
eurjchem-1000	64	25	for	for	ADP
eurjchem-1000	64	26	sildenafil	sildenafil	NOUN
eurjchem-1000	64	27	citrate	citrate	NOUN
eurjchem-1000	64	28	.	.	PUNCT
eurjchem-1000	65	1	detection	detection	NOUN
eurjchem-1000	65	2	of	of	ADP
eurjchem-1000	65	3	the	the	DET
eurjchem-1000	65	4	ions	ion	NOUN
eurjchem-1000	65	5	was	be	AUX
eurjchem-1000	65	6	carried	carry	VERB
eurjchem-1000	65	7	out	out	ADP
eurjchem-1000	65	8	in	in	ADP
eurjchem-1000	65	9	the	the	DET
eurjchem-1000	65	10	multiple‐reaction	multiple‐reaction	NOUN
eurjchem-1000	65	11	monitoring	monitor	VERB
eurjchem-1000	65	12	mode	mode	NOUN
eurjchem-1000	65	13	(	(	PUNCT
eurjchem-1000	65	14	mrm	mrm	PROPN
eurjchem-1000	65	15	)	)	PUNCT
eurjchem-1000	65	16	,	,	PUNCT
eurjchem-1000	65	17	by	by	ADP
eurjchem-1000	65	18	monitoring	monitor	VERB
eurjchem-1000	65	19	m	m	NOUN
eurjchem-1000	65	20	/	/	SYM
eurjchem-1000	65	21	z	z	PROPN
eurjchem-1000	65	22	749.62/82.87	749.62/82.87	NUM
eurjchem-1000	65	23	for	for	ADP
eurjchem-1000	65	24	azithromycin	azithromycin	NOUN
eurjchem-1000	65	25	ion	ion	NOUN
eurjchem-1000	65	26	and	and	CCONJ
eurjchem-1000	65	27	m	m	PROPN
eurjchem-1000	65	28	/	/	SYM
eurjchem-1000	65	29	z	z	PROPN
eurjchem-1000	65	30	475.34/99.75	475.34/99.75	PROPN
eurjchem-1000	65	31	for	for	ADP
eurjchem-1000	65	32	sildenafil	sildenafil	NOUN
eurjchem-1000	65	33	citrate	citrate	NOUN
eurjchem-1000	65	34	ion	ion	NOUN
eurjchem-1000	65	35	(	(	PUNCT
eurjchem-1000	65	36	is	be	AUX
eurjchem-1000	65	37	)	)	PUNCT
eurjchem-1000	65	38	.	.	PUNCT
eurjchem-1000	66	1	data	datum	NOUN
eurjchem-1000	66	2	acquisition	acquisition	NOUN
eurjchem-1000	66	3	and	and	CCONJ
eurjchem-1000	66	4	data	datum	NOUN
eurjchem-1000	66	5	integration	integration	NOUN
eurjchem-1000	66	6	were	be	AUX
eurjchem-1000	66	7	done	do	VERB
eurjchem-1000	66	8	using	use	VERB
eurjchem-1000	66	9	empower	empower	NOUN
eurjchem-1000	66	10	™	™	PROPN
eurjchem-1000	66	11	ver	ver	NOUN
eurjchem-1000	66	12	.	.	PROPN
eurjchem-1000	66	13	2	2	NUM
eurjchem-1000	66	14	cds	cd	NOUN
eurjchem-1000	66	15	software	software	NOUN
eurjchem-1000	66	16	solutions	solution	NOUN
eurjchem-1000	66	17	.	.	PUNCT
eurjchem-1000	67	1	2.4	2.4	NUM
eurjchem-1000	67	2	.	.	PUNCT
eurjchem-1000	67	3	preparation	preparation	NOUN
eurjchem-1000	67	4	of	of	ADP
eurjchem-1000	67	5	stock	stock	NOUN
eurjchem-1000	67	6	solutions	solution	NOUN
eurjchem-1000	67	7	,	,	PUNCT
eurjchem-1000	67	8	secondary	secondary	ADJ
eurjchem-1000	67	9	and	and	CCONJ
eurjchem-1000	67	10	working	working	ADJ
eurjchem-1000	67	11	solutions	solution	NOUN
eurjchem-1000	67	12	2.4.1	2.4.1	NUM
eurjchem-1000	67	13	.	.	PUNCT
eurjchem-1000	68	1	stock	stock	NOUN
eurjchem-1000	68	2	solution	solution	NOUN
eurjchem-1000	68	3	of	of	ADP
eurjchem-1000	68	4	azithromycin	azithromycin	PROPN
eurjchem-1000	68	5	for	for	ADP
eurjchem-1000	68	6	calibration	calibration	NOUN
eurjchem-1000	68	7	and	and	CCONJ
eurjchem-1000	68	8	quality	quality	NOUN
eurjchem-1000	68	9	control	control	NOUN
eurjchem-1000	68	10	a	a	DET
eurjchem-1000	68	11	stock	stock	NOUN
eurjchem-1000	68	12	standard	standard	ADJ
eurjchem-1000	68	13	solution	solution	NOUN
eurjchem-1000	68	14	of	of	ADP
eurjchem-1000	68	15	azithromycin	azithromycin	PROPN
eurjchem-1000	68	16	(	(	PUNCT
eurjchem-1000	68	17	100	100	NUM
eurjchem-1000	68	18	μg	μg	NOUN
eurjchem-1000	68	19	/	/	SYM
eurjchem-1000	68	20	ml	ml	NOUN
eurjchem-1000	68	21	)	)	PUNCT
eurjchem-1000	68	22	was	be	AUX
eurjchem-1000	68	23	prepared	prepare	VERB
eurjchem-1000	68	24	by	by	ADP
eurjchem-1000	68	25	accurate	accurate	ADJ
eurjchem-1000	68	26	weighing	weighing	NOUN
eurjchem-1000	68	27	and	and	CCONJ
eurjchem-1000	68	28	transferring	transfer	VERB
eurjchem-1000	68	29	10	10	NUM
eurjchem-1000	68	30	mg	mg	ADP
eurjchem-1000	68	31	of	of	ADP
eurjchem-1000	68	32	azithromycin	azithromycin	NOUN
eurjchem-1000	68	33	into	into	ADP
eurjchem-1000	68	34	a	a	DET
eurjchem-1000	68	35	100	100	NUM
eurjchem-1000	68	36	ml	ml	NOUN
eurjchem-1000	68	37	volumetric	volumetric	ADJ
eurjchem-1000	68	38	flask	flask	NOUN
eurjchem-1000	68	39	and	and	CCONJ
eurjchem-1000	68	40	diluting	dilute	VERB
eurjchem-1000	68	41	to	to	PART
eurjchem-1000	68	42	volume	volume	VERB
eurjchem-1000	68	43	with	with	ADP
eurjchem-1000	68	44	the	the	DET
eurjchem-1000	68	45	mobile	mobile	ADJ
eurjchem-1000	68	46	phase	phase	NOUN
eurjchem-1000	68	47	.	.	PUNCT
eurjchem-1000	69	1	2.4.2	2.4.2	NUM
eurjchem-1000	69	2	.	.	PUNCT
eurjchem-1000	69	3	working	work	VERB
eurjchem-1000	69	4	solutions	solution	NOUN
eurjchem-1000	69	5	of	of	ADP
eurjchem-1000	69	6	azithromycin	azithromycin	NOUN
eurjchem-1000	69	7	different	different	ADJ
eurjchem-1000	69	8	working	work	VERB
eurjchem-1000	69	9	standard	standard	ADJ
eurjchem-1000	69	10	solutions	solution	NOUN
eurjchem-1000	69	11	of	of	ADP
eurjchem-1000	69	12	azithromycin	azithromycin	PROPN
eurjchem-1000	69	13	(	(	PUNCT
eurjchem-1000	69	14	b	b	NOUN
eurjchem-1000	69	15	,	,	PUNCT
eurjchem-1000	69	16	c	c	NOUN
eurjchem-1000	69	17	,	,	PUNCT
eurjchem-1000	69	18	d	d	NOUN
eurjchem-1000	69	19	,	,	PUNCT
eurjchem-1000	69	20	e	e	NOUN
eurjchem-1000	69	21	and	and	CCONJ
eurjchem-1000	69	22	f	f	X
eurjchem-1000	69	23	)	)	PUNCT
eurjchem-1000	69	24	were	be	AUX
eurjchem-1000	69	25	prepared	prepare	VERB
eurjchem-1000	69	26	by	by	ADP
eurjchem-1000	69	27	transferring	transfer	VERB
eurjchem-1000	69	28	(	(	PUNCT
eurjchem-1000	69	29	10	10	NUM
eurjchem-1000	69	30	ml	ml	NOUN
eurjchem-1000	69	31	,	,	PUNCT
eurjchem-1000	69	32	1	1	NUM
eurjchem-1000	69	33	ml	ml	NOUN
eurjchem-1000	69	34	,	,	PUNCT
eurjchem-1000	69	35	100	100	NUM
eurjchem-1000	69	36	µl	µl	ADP
eurjchem-1000	69	37	,	,	PUNCT
eurjchem-1000	69	38	10	10	NUM
eurjchem-1000	69	39	µl	µl	ADP
eurjchem-1000	69	40	and	and	CCONJ
eurjchem-1000	69	41	1	1	NUM
eurjchem-1000	69	42	µl	µl	NOUN
eurjchem-1000	69	43	,	,	PUNCT
eurjchem-1000	69	44	respectively	respectively	ADV
eurjchem-1000	69	45	)	)	PUNCT
eurjchem-1000	69	46	of	of	ADP
eurjchem-1000	69	47	stock	stock	NOUN
eurjchem-1000	69	48	solution	solution	NOUN
eurjchem-1000	69	49	each	each	PRON
eurjchem-1000	69	50	into	into	ADP
eurjchem-1000	69	51	a	a	DET
eurjchem-1000	69	52	100	100	NUM
eurjchem-1000	69	53	ml	ml	NOUN
eurjchem-1000	69	54	volumetric	volumetric	ADJ
eurjchem-1000	69	55	flask	flask	NOUN
eurjchem-1000	69	56	and	and	CCONJ
eurjchem-1000	69	57	diluting	dilute	VERB
eurjchem-1000	69	58	to	to	PART
eurjchem-1000	69	59	volume	volume	VERB
eurjchem-1000	69	60	with	with	ADP
eurjchem-1000	69	61	mobile	mobile	ADJ
eurjchem-1000	69	62	phase	phase	NOUN
eurjchem-1000	69	63	to	to	PART
eurjchem-1000	69	64	give	give	VERB
eurjchem-1000	69	65	a	a	DET
eurjchem-1000	69	66	final	final	ADJ
eurjchem-1000	69	67	concentrations	concentration	NOUN
eurjchem-1000	69	68	of	of	ADP
eurjchem-1000	69	69	(	(	PUNCT
eurjchem-1000	69	70	10	10	NUM
eurjchem-1000	69	71	μg	μg	NOUN
eurjchem-1000	69	72	/	/	SYM
eurjchem-1000	69	73	ml	ml	NOUN
eurjchem-1000	69	74	,	,	PUNCT
eurjchem-1000	69	75	1	1	NUM
eurjchem-1000	69	76	μg	μg	PROPN
eurjchem-1000	69	77	/	/	SYM
eurjchem-1000	69	78	ml	ml	NOUN
eurjchem-1000	69	79	,	,	PUNCT
eurjchem-1000	69	80	100	100	NUM
eurjchem-1000	69	81	ng	ng	NOUN
eurjchem-1000	69	82	/	/	SYM
eurjchem-1000	69	83	ml	ml	PROPN
eurjchem-1000	69	84	,	,	PUNCT
eurjchem-1000	69	85	10	10	NUM
eurjchem-1000	69	86	ng	ng	NOUN
eurjchem-1000	69	87	/	/	SYM
eurjchem-1000	69	88	ml	ml	NOUN
eurjchem-1000	69	89	and	and	CCONJ
eurjchem-1000	69	90	1	1	NUM
eurjchem-1000	69	91	ng	ng	PROPN
eurjchem-1000	69	92	/	/	SYM
eurjchem-1000	69	93	ml	ml	NOUN
eurjchem-1000	69	94	,	,	PUNCT
eurjchem-1000	69	95	respectively	respectively	ADV
eurjchem-1000	69	96	)	)	PUNCT
eurjchem-1000	69	97	.	.	PUNCT
eurjchem-1000	70	1	2.4.3	2.4.3	X
eurjchem-1000	70	2	.	.	PUNCT
eurjchem-1000	70	3	stock	stock	NOUN
eurjchem-1000	70	4	solution	solution	NOUN
eurjchem-1000	70	5	of	of	ADP
eurjchem-1000	70	6	internal	internal	ADJ
eurjchem-1000	70	7	standard	standard	NOUN
eurjchem-1000	70	8	for	for	ADP
eurjchem-1000	70	9	calibration	calibration	NOUN
eurjchem-1000	70	10	and	and	CCONJ
eurjchem-1000	70	11	quality	quality	NOUN
eurjchem-1000	70	12	control	control	NOUN
eurjchem-1000	70	13	a	a	DET
eurjchem-1000	70	14	stock	stock	NOUN
eurjchem-1000	70	15	standard	standard	ADJ
eurjchem-1000	70	16	solution	solution	NOUN
eurjchem-1000	70	17	of	of	ADP
eurjchem-1000	70	18	sildenafil	sildenafil	NOUN
eurjchem-1000	70	19	citrate	citrate	NOUN
eurjchem-1000	70	20	(	(	PUNCT
eurjchem-1000	70	21	100	100	NUM
eurjchem-1000	70	22	µg	µg	ADJ
eurjchem-1000	70	23	/	/	SYM
eurjchem-1000	70	24	ml	ml	NOUN
eurjchem-1000	70	25	)	)	PUNCT
eurjchem-1000	70	26	was	be	AUX
eurjchem-1000	70	27	prepared	prepare	VERB
eurjchem-1000	70	28	by	by	ADP
eurjchem-1000	70	29	accurately	accurately	ADV
eurjchem-1000	70	30	weighing	weigh	VERB
eurjchem-1000	70	31	and	and	CCONJ
eurjchem-1000	70	32	transferring	transfer	VERB
eurjchem-1000	70	33	10	10	NUM
eurjchem-1000	70	34	mg	mg	NOUN
eurjchem-1000	70	35	of	of	ADP
eurjchem-1000	70	36	sildenafil	sildenafil	NOUN
eurjchem-1000	70	37	citrate	citrate	NOUN
eurjchem-1000	70	38	into	into	ADP
eurjchem-1000	70	39	a	a	DET
eurjchem-1000	70	40	100	100	NUM
eurjchem-1000	70	41	ml	ml	NOUN
eurjchem-1000	70	42	volumetric	volumetric	ADJ
eurjchem-1000	70	43	flask	flask	NOUN
eurjchem-1000	70	44	and	and	CCONJ
eurjchem-1000	70	45	diluting	dilute	VERB
eurjchem-1000	70	46	to	to	PART
eurjchem-1000	70	47	volume	volume	VERB
eurjchem-1000	70	48	with	with	ADP
eurjchem-1000	70	49	mobile	mobile	ADJ
eurjchem-1000	70	50	phase	phase	NOUN
eurjchem-1000	70	51	.	.	PUNCT
eurjchem-1000	71	1	2.4.4	2.4.4	NUM
eurjchem-1000	71	2	.	.	PUNCT
eurjchem-1000	71	3	working	work	VERB
eurjchem-1000	71	4	solution	solution	NOUN
eurjchem-1000	71	5	of	of	ADP
eurjchem-1000	71	6	internal	internal	ADJ
eurjchem-1000	71	7	standard	standard	NOUN
eurjchem-1000	71	8	a	a	DET
eurjchem-1000	71	9	working	work	VERB
eurjchem-1000	71	10	standard	standard	ADJ
eurjchem-1000	71	11	solution	solution	NOUN
eurjchem-1000	71	12	of	of	ADP
eurjchem-1000	71	13	sildenafil	sildenafil	NOUN
eurjchem-1000	71	14	citrate	citrate	NOUN
eurjchem-1000	71	15	(	(	PUNCT
eurjchem-1000	71	16	0.5	0.5	NUM
eurjchem-1000	71	17	µg	µg	NOUN
eurjchem-1000	71	18	/	/	SYM
eurjchem-1000	71	19	ml	ml	NOUN
eurjchem-1000	71	20	)	)	PUNCT
eurjchem-1000	71	21	was	be	AUX
eurjchem-1000	71	22	prepared	prepare	VERB
eurjchem-1000	71	23	by	by	ADP
eurjchem-1000	71	24	transferring	transfer	VERB
eurjchem-1000	71	25	0.5	0.5	NUM
eurjchem-1000	71	26	ml	ml	NOUN
eurjchem-1000	71	27	of	of	ADP
eurjchem-1000	71	28	stock	stock	NOUN
eurjchem-1000	71	29	solution	solution	NOUN
eurjchem-1000	71	30	into	into	ADP
eurjchem-1000	71	31	a	a	DET
eurjchem-1000	71	32	100	100	NUM
eurjchem-1000	71	33	ml	ml	NOUN
eurjchem-1000	71	34	volumetric	volumetric	ADJ
eurjchem-1000	71	35	flask	flask	NOUN
eurjchem-1000	71	36	and	and	CCONJ
eurjchem-1000	71	37	diluting	dilute	VERB
eurjchem-1000	71	38	to	to	PART
eurjchem-1000	71	39	volume	volume	VERB
eurjchem-1000	71	40	with	with	ADP
eurjchem-1000	71	41	mobile	mobile	ADJ
eurjchem-1000	71	42	phase	phase	NOUN
eurjchem-1000	71	43	.	.	PUNCT
eurjchem-1000	72	1	human	human	ADJ
eurjchem-1000	72	2	plasma	plasma	NOUN
eurjchem-1000	72	3	was	be	AUX
eurjchem-1000	72	4	chromatographed	chromatographe	VERB
eurjchem-1000	72	5	prior	prior	ADV
eurjchem-1000	72	6	to	to	ADP
eurjchem-1000	72	7	use	use	NOUN
eurjchem-1000	72	8	to	to	PART
eurjchem-1000	72	9	determine	determine	VERB
eurjchem-1000	72	10	possible	possible	ADJ
eurjchem-1000	72	11	interference	interference	NOUN
eurjchem-1000	72	12	with	with	ADP
eurjchem-1000	72	13	azithromycin	azithromycin	NOUN
eurjchem-1000	72	14	or	or	CCONJ
eurjchem-1000	72	15	internal	internal	ADJ
eurjchem-1000	72	16	standard	standard	NOUN
eurjchem-1000	72	17	.	.	PUNCT
eurjchem-1000	73	1	younes	younes	PROPN
eurjchem-1000	73	2	and	and	CCONJ
eurjchem-1000	73	3	el‐kady	el‐kady	PROPN
eurjchem-1000	73	4	/	/	SYM
eurjchem-1000	73	5	european	european	PROPN
eurjchem-1000	73	6	journal	journal	PROPN
eurjchem-1000	73	7	of	of	ADP
eurjchem-1000	73	8	chemistry	chemistry	NOUN
eurjchem-1000	73	9	5	5	NUM
eurjchem-1000	73	10	(	(	PUNCT
eurjchem-1000	73	11	2	2	NUM
eurjchem-1000	73	12	)	)	PUNCT
eurjchem-1000	73	13	(	(	PUNCT
eurjchem-1000	73	14	2014	2014	NUM
eurjchem-1000	73	15	)	)	PUNCT
eurjchem-1000	73	16	241‐246	241‐246	NUM
eurjchem-1000	73	17	243	243	NUM
eurjchem-1000	73	18	table	table	NOUN
eurjchem-1000	73	19	1	1	NUM
eurjchem-1000	73	20	.	.	PUNCT
eurjchem-1000	74	1	the	the	DET
eurjchem-1000	74	2	optimum	optimum	ADJ
eurjchem-1000	74	3	multiple	multiple	ADJ
eurjchem-1000	74	4	reaction	reaction	NOUN
eurjchem-1000	74	5	mode	mode	NOUN
eurjchem-1000	74	6	parameters	parameter	NOUN
eurjchem-1000	74	7	for	for	ADP
eurjchem-1000	74	8	both	both	DET
eurjchem-1000	74	9	drug	drug	NOUN
eurjchem-1000	74	10	and	and	CCONJ
eurjchem-1000	74	11	is	be	AUX
eurjchem-1000	74	12	.	.	PUNCT
eurjchem-1000	75	1	no	no	DET
eurjchem-1000	75	2	drug	drug	NOUN
eurjchem-1000	75	3	/	/	PUNCT
eurjchem-1000	75	4	is	be	AUX
eurjchem-1000	75	5	precursor	precursor	NOUN
eurjchem-1000	75	6	(	(	PUNCT
eurjchem-1000	75	7	da	da	NOUN
eurjchem-1000	75	8	)	)	PUNCT
eurjchem-1000	75	9	product	product	NOUN
eurjchem-1000	75	10	(	(	PUNCT
eurjchem-1000	75	11	da	da	NOUN
eurjchem-1000	75	12	)	)	PUNCT
eurjchem-1000	75	13	dwell	dwell	NOUN
eurjchem-1000	75	14	(	(	PUNCT
eurjchem-1000	75	15	sec	sec	PROPN
eurjchem-1000	75	16	)	)	PUNCT
eurjchem-1000	75	17	cone	cone	NOUN
eurjchem-1000	75	18	voltage	voltage	NOUN
eurjchem-1000	75	19	(	(	PUNCT
eurjchem-1000	75	20	v	v	NOUN
eurjchem-1000	75	21	)	)	PUNCT
eurjchem-1000	75	22	collision	collision	NOUN
eurjchem-1000	75	23	energy	energy	NOUN
eurjchem-1000	75	24	(	(	PUNCT
eurjchem-1000	75	25	v	v	NOUN
eurjchem-1000	75	26	)	)	PUNCT
eurjchem-1000	75	27	1	1	NUM
eurjchem-1000	75	28	sildenafil	sildenafil	NOUN
eurjchem-1000	75	29	(	(	PUNCT
eurjchem-1000	75	30	is	be	AUX
eurjchem-1000	75	31	)	)	PUNCT
eurjchem-1000	75	32	475.34	475.34	NUM
eurjchem-1000	75	33	99.75	99.75	NUM
eurjchem-1000	75	34	0.100	0.100	NUM
eurjchem-1000	75	35	50	50	NUM
eurjchem-1000	75	36	30	30	NUM
eurjchem-1000	75	37	2	2	NUM
eurjchem-1000	75	38	azithromycin	azithromycin	NOUN
eurjchem-1000	75	39	749.62	749.62	NUM
eurjchem-1000	75	40	82.87	82.87	NUM
eurjchem-1000	75	41	0.100	0.100	NUM
eurjchem-1000	75	42	40	40	NUM
eurjchem-1000	75	43	38	38	NUM
eurjchem-1000	75	44	no	no	DET
eurjchem-1000	75	45	significant	significant	ADJ
eurjchem-1000	75	46	interferences	interference	NOUN
eurjchem-1000	75	47	were	be	AUX
eurjchem-1000	75	48	observed	observe	VERB
eurjchem-1000	75	49	in	in	ADP
eurjchem-1000	75	50	the	the	DET
eurjchem-1000	75	51	lots	lot	NOUN
eurjchem-1000	75	52	of	of	ADP
eurjchem-1000	75	53	human	human	ADJ
eurjchem-1000	75	54	plasma	plasma	NOUN
eurjchem-1000	75	55	used	use	VERB
eurjchem-1000	75	56	for	for	ADP
eurjchem-1000	75	57	the	the	DET
eurjchem-1000	75	58	preparation	preparation	NOUN
eurjchem-1000	75	59	of	of	ADP
eurjchem-1000	75	60	calibration	calibration	NOUN
eurjchem-1000	75	61	standards	standard	NOUN
eurjchem-1000	75	62	and	and	CCONJ
eurjchem-1000	75	63	quality	quality	NOUN
eurjchem-1000	75	64	control	control	NOUN
eurjchem-1000	75	65	samples	sample	NOUN
eurjchem-1000	75	66	.	.	PUNCT
eurjchem-1000	76	1	2.5	2.5	NUM
eurjchem-1000	76	2	.	.	PUNCT
eurjchem-1000	77	1	preparation	preparation	NOUN
eurjchem-1000	77	2	of	of	ADP
eurjchem-1000	77	3	calibration	calibration	NOUN
eurjchem-1000	77	4	curve	curve	NOUN
eurjchem-1000	77	5	and	and	CCONJ
eurjchem-1000	77	6	quality	quality	NOUN
eurjchem-1000	77	7	control	control	NOUN
eurjchem-1000	77	8	solutions	solution	NOUN
eurjchem-1000	77	9	standard	standard	ADJ
eurjchem-1000	77	10	curve	curve	NOUN
eurjchem-1000	77	11	was	be	AUX
eurjchem-1000	77	12	produced	produce	VERB
eurjchem-1000	77	13	by	by	ADP
eurjchem-1000	77	14	preparing	prepare	VERB
eurjchem-1000	77	15	six	six	NUM
eurjchem-1000	77	16	plasma	plasma	NOUN
eurjchem-1000	77	17	standards	standard	NOUN
eurjchem-1000	77	18	over	over	ADP
eurjchem-1000	77	19	the	the	DET
eurjchem-1000	77	20	range	range	NOUN
eurjchem-1000	77	21	of	of	ADP
eurjchem-1000	77	22	5.0‐1500.0	5.0‐1500.0	NUM
eurjchem-1000	77	23	ng	ng	NOUN
eurjchem-1000	77	24	/	/	SYM
eurjchem-1000	77	25	ml	ml	NOUN
eurjchem-1000	77	26	for	for	ADP
eurjchem-1000	77	27	azithromycin	azithromycin	PROPN
eurjchem-1000	77	28	.	.	PUNCT
eurjchem-1000	78	1	standards	standard	NOUN
eurjchem-1000	78	2	were	be	AUX
eurjchem-1000	78	3	prepared	prepare	VERB
eurjchem-1000	78	4	in	in	ADP
eurjchem-1000	78	5	triplicates	triplicate	NOUN
eurjchem-1000	78	6	.	.	PUNCT
eurjchem-1000	79	1	similarly	similarly	ADV
eurjchem-1000	79	2	,	,	PUNCT
eurjchem-1000	79	3	quality	quality	NOUN
eurjchem-1000	79	4	control	control	NOUN
eurjchem-1000	79	5	(	(	PUNCT
eurjchem-1000	79	6	qc	qc	PROPN
eurjchem-1000	79	7	)	)	PUNCT
eurjchem-1000	79	8	samples	sample	NOUN
eurjchem-1000	79	9	were	be	AUX
eurjchem-1000	79	10	also	also	ADV
eurjchem-1000	79	11	prepared	prepare	VERB
eurjchem-1000	79	12	as	as	ADP
eurjchem-1000	79	13	a	a	DET
eurjchem-1000	79	14	bulk	bulk	NOUN
eurjchem-1000	79	15	based	base	VERB
eurjchem-1000	79	16	on	on	ADP
eurjchem-1000	79	17	an	an	DET
eurjchem-1000	79	18	independent	independent	ADJ
eurjchem-1000	79	19	weighing	weighing	NOUN
eurjchem-1000	79	20	of	of	ADP
eurjchem-1000	79	21	standard	standard	ADJ
eurjchem-1000	79	22	drug	drug	NOUN
eurjchem-1000	79	23	,	,	PUNCT
eurjchem-1000	79	24	at	at	ADP
eurjchem-1000	79	25	concentrations	concentration	NOUN
eurjchem-1000	79	26	of	of	ADP
eurjchem-1000	79	27	5.0	5.0	NUM
eurjchem-1000	79	28	(	(	PUNCT
eurjchem-1000	79	29	lower	low	ADJ
eurjchem-1000	79	30	limit	limit	NOUN
eurjchem-1000	79	31	of	of	ADP
eurjchem-1000	79	32	quantitation	quantitation	NOUN
eurjchem-1000	79	33	,	,	PUNCT
eurjchem-1000	79	34	lloq	lloq	PROPN
eurjchem-1000	79	35	)	)	PUNCT
eurjchem-1000	79	36	,	,	PUNCT
eurjchem-1000	79	37	10.0	10.0	NUM
eurjchem-1000	79	38	(	(	PUNCT
eurjchem-1000	79	39	low	low	ADJ
eurjchem-1000	79	40	;	;	PUNCT
eurjchem-1000	79	41	low	low	ADJ
eurjchem-1000	79	42	quality	quality	NOUN
eurjchem-1000	79	43	control	control	NOUN
eurjchem-1000	79	44	,	,	PUNCT
eurjchem-1000	79	45	qcl	qcl	NOUN
eurjchem-1000	79	46	)	)	PUNCT
eurjchem-1000	79	47	,	,	PUNCT
eurjchem-1000	79	48	400.0	400.0	NUM
eurjchem-1000	79	49	(	(	PUNCT
eurjchem-1000	79	50	middle	middle	ADJ
eurjchem-1000	79	51	;	;	PUNCT
eurjchem-1000	79	52	medium	medium	ADJ
eurjchem-1000	79	53	quality	quality	NOUN
eurjchem-1000	79	54	control	control	NOUN
eurjchem-1000	79	55	,	,	PUNCT
eurjchem-1000	79	56	qcm	qcm	PROPN
eurjchem-1000	79	57	)	)	PUNCT
eurjchem-1000	79	58	and	and	CCONJ
eurjchem-1000	79	59	1200.0	1200.0	NUM
eurjchem-1000	79	60	ng	ng	NOUN
eurjchem-1000	79	61	/	/	SYM
eurjchem-1000	79	62	ml	ml	PROPN
eurjchem-1000	79	63	(	(	PUNCT
eurjchem-1000	79	64	high	high	ADJ
eurjchem-1000	79	65	;	;	PUNCT
eurjchem-1000	79	66	high	high	ADJ
eurjchem-1000	79	67	quality	quality	NOUN
eurjchem-1000	79	68	control	control	NOUN
eurjchem-1000	79	69	,	,	PUNCT
eurjchem-1000	79	70	qch	qch	PROPN
eurjchem-1000	79	71	)	)	PUNCT
eurjchem-1000	79	72	as	as	ADP
eurjchem-1000	79	73	a	a	DET
eurjchem-1000	79	74	single	single	ADJ
eurjchem-1000	79	75	batch	batch	NOUN
eurjchem-1000	79	76	at	at	ADP
eurjchem-1000	79	77	each	each	DET
eurjchem-1000	79	78	concentration	concentration	NOUN
eurjchem-1000	79	79	.	.	PUNCT
eurjchem-1000	80	1	each	each	DET
eurjchem-1000	80	2	calibrations	calibration	NOUN
eurjchem-1000	80	3	or	or	CCONJ
eurjchem-1000	80	4	qc	qc	PROPN
eurjchem-1000	80	5	solution	solution	NOUN
eurjchem-1000	80	6	was	be	AUX
eurjchem-1000	80	7	prepared	prepare	VERB
eurjchem-1000	80	8	by	by	ADP
eurjchem-1000	80	9	spiking	spike	VERB
eurjchem-1000	80	10	50	50	NUM
eurjchem-1000	80	11	μl	μl	ADP
eurjchem-1000	80	12	of	of	ADP
eurjchem-1000	80	13	the	the	DET
eurjchem-1000	80	14	corresponding	correspond	VERB
eurjchem-1000	80	15	stock	stock	NOUN
eurjchem-1000	80	16	solution	solution	NOUN
eurjchem-1000	80	17	into	into	ADP
eurjchem-1000	80	18	450	450	NUM
eurjchem-1000	80	19	μl	μl	ADP
eurjchem-1000	80	20	of	of	ADP
eurjchem-1000	80	21	human	human	ADJ
eurjchem-1000	80	22	plasma	plasma	NOUN
eurjchem-1000	80	23	,	,	PUNCT
eurjchem-1000	80	24	then	then	ADV
eurjchem-1000	80	25	100	100	NUM
eurjchem-1000	80	26	µl	µl	NOUN
eurjchem-1000	80	27	of	of	ADP
eurjchem-1000	80	28	na2co3	na2co3	NOUN
eurjchem-1000	80	29	(	(	PUNCT
eurjchem-1000	80	30	30	30	NUM
eurjchem-1000	80	31	%	%	NOUN
eurjchem-1000	80	32	,	,	PUNCT
eurjchem-1000	80	33	w	w	NOUN
eurjchem-1000	80	34	:	:	SYM
eurjchem-1000	80	35	v	v	NOUN
eurjchem-1000	80	36	)	)	PUNCT
eurjchem-1000	80	37	was	be	AUX
eurjchem-1000	80	38	spiked	spike	VERB
eurjchem-1000	80	39	.	.	PUNCT
eurjchem-1000	81	1	then	then	ADV
eurjchem-1000	81	2	extraction	extraction	NOUN
eurjchem-1000	81	3	with	with	ADP
eurjchem-1000	81	4	6	6	NUM
eurjchem-1000	81	5	ml	ml	NOUN
eurjchem-1000	81	6	tert‐butyl	tert‐butyl	ADP
eurjchem-1000	81	7	methyl	methyl	NOUN
eurjchem-1000	81	8	ether	ether	NOUN
eurjchem-1000	81	9	was	be	AUX
eurjchem-1000	81	10	done	do	VERB
eurjchem-1000	81	11	.	.	PUNCT
eurjchem-1000	82	1	the	the	DET
eurjchem-1000	82	2	mixture	mixture	NOUN
eurjchem-1000	82	3	was	be	AUX
eurjchem-1000	82	4	vortexed	vortexe	VERB
eurjchem-1000	82	5	for	for	ADP
eurjchem-1000	82	6	thirty	thirty	NUM
eurjchem-1000	82	7	seconds	second	NOUN
eurjchem-1000	82	8	and	and	CCONJ
eurjchem-1000	82	9	centrifuged	centrifuge	VERB
eurjchem-1000	82	10	at	at	ADP
eurjchem-1000	82	11	4000	4000	NUM
eurjchem-1000	82	12	rpm	rpm	NOUN
eurjchem-1000	82	13	for	for	ADP
eurjchem-1000	82	14	five	five	NUM
eurjchem-1000	82	15	minutes	minute	NOUN
eurjchem-1000	82	16	.	.	PUNCT
eurjchem-1000	83	1	the	the	DET
eurjchem-1000	83	2	organic	organic	ADJ
eurjchem-1000	83	3	layer	layer	NOUN
eurjchem-1000	83	4	was	be	AUX
eurjchem-1000	83	5	then	then	ADV
eurjchem-1000	83	6	separated	separate	VERB
eurjchem-1000	83	7	and	and	CCONJ
eurjchem-1000	83	8	evaporated	evaporate	VERB
eurjchem-1000	83	9	in	in	ADP
eurjchem-1000	83	10	epindorff	epindorff	NOUN
eurjchem-1000	83	11	evaporator	evaporator	NOUN
eurjchem-1000	83	12	then	then	ADV
eurjchem-1000	83	13	the	the	DET
eurjchem-1000	83	14	residue	residue	NOUN
eurjchem-1000	83	15	was	be	AUX
eurjchem-1000	83	16	reconstituted	reconstitute	VERB
eurjchem-1000	83	17	with	with	ADP
eurjchem-1000	83	18	250	250	NUM
eurjchem-1000	83	19	µl	µl	NOUN
eurjchem-1000	83	20	of	of	ADP
eurjchem-1000	83	21	is	be	AUX
eurjchem-1000	83	22	dissolved	dissolve	VERB
eurjchem-1000	83	23	in	in	ADP
eurjchem-1000	83	24	mobile	mobile	ADJ
eurjchem-1000	83	25	phase	phase	NOUN
eurjchem-1000	83	26	and	and	CCONJ
eurjchem-1000	83	27	injected	inject	VERB
eurjchem-1000	83	28	.	.	PUNCT
eurjchem-1000	84	1	2.6	2.6	NUM
eurjchem-1000	84	2	.	.	PUNCT
eurjchem-1000	85	1	bio‐analytical	bio‐analytical	PROPN
eurjchem-1000	85	2	method	method	PROPN
eurjchem-1000	85	3	validation	validation	NOUN
eurjchem-1000	85	4	the	the	DET
eurjchem-1000	85	5	method	method	NOUN
eurjchem-1000	85	6	was	be	AUX
eurjchem-1000	85	7	validated	validate	VERB
eurjchem-1000	85	8	in	in	ADP
eurjchem-1000	85	9	accordance	accordance	NOUN
eurjchem-1000	85	10	with	with	ADP
eurjchem-1000	85	11	international	international	ADJ
eurjchem-1000	85	12	regulations	regulation	NOUN
eurjchem-1000	85	13	[	[	X
eurjchem-1000	85	14	30	30	NUM
eurjchem-1000	85	15	]	]	PUNCT
eurjchem-1000	85	16	.	.	PUNCT
eurjchem-1000	86	1	the	the	DET
eurjchem-1000	86	2	parameters	parameter	NOUN
eurjchem-1000	86	3	determined	determine	VERB
eurjchem-1000	86	4	were	be	AUX
eurjchem-1000	86	5	selectivity	selectivity	NOUN
eurjchem-1000	86	6	,	,	PUNCT
eurjchem-1000	86	7	specificity	specificity	NOUN
eurjchem-1000	86	8	,	,	PUNCT
eurjchem-1000	86	9	matrix	matrix	NOUN
eurjchem-1000	86	10	effect	effect	NOUN
eurjchem-1000	86	11	,	,	PUNCT
eurjchem-1000	86	12	linearity	linearity	NOUN
eurjchem-1000	86	13	,	,	PUNCT
eurjchem-1000	86	14	precision	precision	NOUN
eurjchem-1000	86	15	,	,	PUNCT
eurjchem-1000	86	16	accuracy	accuracy	NOUN
eurjchem-1000	86	17	,	,	PUNCT
eurjchem-1000	86	18	recovery	recovery	NOUN
eurjchem-1000	86	19	,	,	PUNCT
eurjchem-1000	86	20	stability	stability	NOUN
eurjchem-1000	86	21	and	and	CCONJ
eurjchem-1000	86	22	dilution	dilution	NOUN
eurjchem-1000	86	23	integrity	integrity	NOUN
eurjchem-1000	86	24	.	.	PUNCT
eurjchem-1000	87	1	3	3	X
eurjchem-1000	87	2	.	.	NOUN
eurjchem-1000	87	3	results	result	NOUN
eurjchem-1000	87	4	and	and	CCONJ
eurjchem-1000	87	5	discussion	discussion	NOUN
eurjchem-1000	87	6	3.1	3.1	NUM
eurjchem-1000	87	7	.	.	PUNCT
eurjchem-1000	88	1	method	method	NOUN
eurjchem-1000	88	2	development	development	NOUN
eurjchem-1000	88	3	3.1.1	3.1.1	NUM
eurjchem-1000	88	4	.	.	PUNCT
eurjchem-1000	89	1	ms‐ms	ms‐ms	PROPN
eurjchem-1000	89	2	tuning	tune	VERB
eurjchem-1000	89	3	mass	mass	ADJ
eurjchem-1000	89	4	parameters	parameter	NOUN
eurjchem-1000	89	5	were	be	AUX
eurjchem-1000	89	6	tuned	tune	VERB
eurjchem-1000	89	7	in	in	ADP
eurjchem-1000	89	8	both	both	CCONJ
eurjchem-1000	89	9	positive	positive	ADJ
eurjchem-1000	89	10	and	and	CCONJ
eurjchem-1000	89	11	negative	negative	ADJ
eurjchem-1000	89	12	ionization	ionization	NOUN
eurjchem-1000	89	13	modes	mode	NOUN
eurjchem-1000	89	14	for	for	ADP
eurjchem-1000	89	15	the	the	DET
eurjchem-1000	89	16	drug	drug	NOUN
eurjchem-1000	89	17	.	.	PUNCT
eurjchem-1000	90	1	good	good	ADJ
eurjchem-1000	90	2	response	response	NOUN
eurjchem-1000	90	3	was	be	AUX
eurjchem-1000	90	4	found	find	VERB
eurjchem-1000	90	5	in	in	ADP
eurjchem-1000	90	6	positive	positive	ADJ
eurjchem-1000	90	7	ionization	ionization	NOUN
eurjchem-1000	90	8	mode	mode	NOUN
eurjchem-1000	90	9	for	for	ADP
eurjchem-1000	90	10	both	both	CCONJ
eurjchem-1000	90	11	the	the	DET
eurjchem-1000	90	12	drug	drug	NOUN
eurjchem-1000	90	13	and	and	CCONJ
eurjchem-1000	90	14	is	be	AUX
eurjchem-1000	90	15	.	.	PUNCT
eurjchem-1000	91	1	the	the	DET
eurjchem-1000	91	2	mrm	mrm	PROPN
eurjchem-1000	91	3	state	state	PROPN
eurjchem-1000	91	4	file	file	NOUN
eurjchem-1000	91	5	parameters	parameter	NOUN
eurjchem-1000	91	6	were	be	AUX
eurjchem-1000	91	7	optimized	optimize	VERB
eurjchem-1000	91	8	to	to	PART
eurjchem-1000	91	9	maximize	maximize	VERB
eurjchem-1000	91	10	the	the	DET
eurjchem-1000	91	11	response	response	NOUN
eurjchem-1000	91	12	for	for	ADP
eurjchem-1000	91	13	both	both	CCONJ
eurjchem-1000	91	14	the	the	DET
eurjchem-1000	91	15	drug	drug	NOUN
eurjchem-1000	91	16	and	and	CCONJ
eurjchem-1000	91	17	is	be	AUX
eurjchem-1000	91	18	as	as	SCONJ
eurjchem-1000	91	19	shown	show	VERB
eurjchem-1000	91	20	in	in	ADP
eurjchem-1000	91	21	table	table	NOUN
eurjchem-1000	91	22	1	1	NUM
eurjchem-1000	91	23	.	.	PUNCT
eurjchem-1000	92	1	the	the	DET
eurjchem-1000	92	2	product	product	NOUN
eurjchem-1000	92	3	ion	ion	NOUN
eurjchem-1000	92	4	mass	mass	NOUN
eurjchem-1000	92	5	spectrum	spectrum	NOUN
eurjchem-1000	92	6	of	of	ADP
eurjchem-1000	92	7	azithromycin	azithromycin	PROPN
eurjchem-1000	92	8	and	and	CCONJ
eurjchem-1000	92	9	is	be	AUX
eurjchem-1000	92	10	are	be	AUX
eurjchem-1000	92	11	presented	present	VERB
eurjchem-1000	92	12	in	in	ADP
eurjchem-1000	92	13	figure	figure	NOUN
eurjchem-1000	92	14	3	3	NUM
eurjchem-1000	92	15	.	.	PUNCT
eurjchem-1000	92	16	figure	figure	NOUN
eurjchem-1000	92	17	3	3	NUM
eurjchem-1000	92	18	.	.	PUNCT
eurjchem-1000	92	19	mass	mass	PROPN
eurjchem-1000	92	20	spectrum	spectrum	NOUN
eurjchem-1000	92	21	of	of	ADP
eurjchem-1000	92	22	pure	pure	ADJ
eurjchem-1000	92	23	azithromycin	azithromycin	NOUN
eurjchem-1000	92	24	and	and	CCONJ
eurjchem-1000	92	25	sildenafil	sildenafil	NOUN
eurjchem-1000	92	26	citrate	citrate	NOUN
eurjchem-1000	92	27	(	(	PUNCT
eurjchem-1000	92	28	is	be	AUX
eurjchem-1000	92	29	)	)	PUNCT
eurjchem-1000	92	30	.	.	PUNCT
eurjchem-1000	93	1	3.1.2	3.1.2	X
eurjchem-1000	93	2	.	.	PUNCT
eurjchem-1000	93	3	chromatographic	chromatographic	ADJ
eurjchem-1000	93	4	separation	separation	NOUN
eurjchem-1000	93	5	separation	separation	NOUN
eurjchem-1000	93	6	was	be	AUX
eurjchem-1000	93	7	attempted	attempt	VERB
eurjchem-1000	93	8	using	use	VERB
eurjchem-1000	93	9	various	various	ADJ
eurjchem-1000	93	10	combinations	combination	NOUN
eurjchem-1000	93	11	of	of	ADP
eurjchem-1000	93	12	acetonitrile	acetonitrile	NOUN
eurjchem-1000	93	13	and	and	CCONJ
eurjchem-1000	93	14	buffers	buffer	NOUN
eurjchem-1000	93	15	with	with	ADP
eurjchem-1000	93	16	varying	vary	VERB
eurjchem-1000	93	17	contents	content	NOUN
eurjchem-1000	93	18	of	of	ADP
eurjchem-1000	93	19	each	each	DET
eurjchem-1000	93	20	component	component	NOUN
eurjchem-1000	93	21	on	on	ADP
eurjchem-1000	93	22	different	different	ADJ
eurjchem-1000	93	23	columns	column	NOUN
eurjchem-1000	93	24	like	like	ADP
eurjchem-1000	93	25	c8	c8	PROPN
eurjchem-1000	93	26	and	and	CCONJ
eurjchem-1000	93	27	c18	c18	NOUN
eurjchem-1000	93	28	of	of	ADP
eurjchem-1000	93	29	different	different	ADJ
eurjchem-1000	93	30	types	type	NOUN
eurjchem-1000	93	31	like	like	ADP
eurjchem-1000	93	32	chromolith	chromolith	NOUN
eurjchem-1000	93	33	,	,	PUNCT
eurjchem-1000	93	34	hypersil	hypersil	NOUN
eurjchem-1000	93	35	,	,	PUNCT
eurjchem-1000	93	36	zorbax	zorbax	NOUN
eurjchem-1000	93	37	,	,	PUNCT
eurjchem-1000	93	38	kromasil	kromasil	NOUN
eurjchem-1000	93	39	and	and	CCONJ
eurjchem-1000	93	40	intertsil	intertsil	NOUN
eurjchem-1000	93	41	etc	etc	X
eurjchem-1000	93	42	.	.	PUNCT
eurjchem-1000	94	1	use	use	NOUN
eurjchem-1000	94	2	of	of	ADP
eurjchem-1000	94	3	0.1	0.1	NUM
eurjchem-1000	94	4	%	%	NOUN
eurjchem-1000	94	5	formic	formic	PROPN
eurjchem-1000	94	6	acid	acid	PROPN
eurjchem-1000	94	7	helped	help	VERB
eurjchem-1000	94	8	in	in	ADP
eurjchem-1000	94	9	achieving	achieve	VERB
eurjchem-1000	94	10	good	good	ADJ
eurjchem-1000	94	11	response	response	NOUN
eurjchem-1000	94	12	for	for	ADP
eurjchem-1000	94	13	ms	ms	NOUN
eurjchem-1000	94	14	detection	detection	NOUN
eurjchem-1000	94	15	by	by	ADP
eurjchem-1000	94	16	facilitating	facilitate	VERB
eurjchem-1000	94	17	ionization	ionization	NOUN
eurjchem-1000	94	18	of	of	ADP
eurjchem-1000	94	19	the	the	DET
eurjchem-1000	94	20	ions	ion	NOUN
eurjchem-1000	94	21	.	.	PUNCT
eurjchem-1000	95	1	a	a	DET
eurjchem-1000	95	2	mobile	mobile	ADJ
eurjchem-1000	95	3	phase	phase	NOUN
eurjchem-1000	95	4	consisting	consist	VERB
eurjchem-1000	95	5	of	of	ADP
eurjchem-1000	95	6	acetonitrile	acetonitrile	NOUN
eurjchem-1000	95	7	and	and	CCONJ
eurjchem-1000	95	8	0.1	0.1	NUM
eurjchem-1000	95	9	%	%	NOUN
eurjchem-1000	95	10	formic	formic	NOUN
eurjchem-1000	95	11	acid	acid	NOUN
eurjchem-1000	95	12	(	(	PUNCT
eurjchem-1000	95	13	80:20	80:20	NUM
eurjchem-1000	95	14	,	,	PUNCT
eurjchem-1000	95	15	v	v	NOUN
eurjchem-1000	95	16	:	:	SYM
eurjchem-1000	95	17	v	v	NOUN
eurjchem-1000	95	18	)	)	PUNCT
eurjchem-1000	95	19	was	be	AUX
eurjchem-1000	95	20	found	find	VERB
eurjchem-1000	95	21	suitable	suitable	ADJ
eurjchem-1000	95	22	for	for	ADP
eurjchem-1000	95	23	both	both	CCONJ
eurjchem-1000	95	24	the	the	DET
eurjchem-1000	95	25	drug	drug	NOUN
eurjchem-1000	95	26	and	and	CCONJ
eurjchem-1000	95	27	is	be	AUX
eurjchem-1000	95	28	.	.	PUNCT
eurjchem-1000	96	1	the	the	DET
eurjchem-1000	96	2	chromatographic	chromatographic	ADJ
eurjchem-1000	96	3	separation	separation	NOUN
eurjchem-1000	96	4	was	be	AUX
eurjchem-1000	96	5	performed	perform	VERB
eurjchem-1000	96	6	at	at	ADP
eurjchem-1000	96	7	room	room	NOUN
eurjchem-1000	96	8	temperature	temperature	NOUN
eurjchem-1000	96	9	on	on	ADP
eurjchem-1000	96	10	waters	water	NOUN
eurjchem-1000	96	11	c18	c18	NOUN
eurjchem-1000	96	12	column	column	NOUN
eurjchem-1000	96	13	(	(	PUNCT
eurjchem-1000	96	14	50	50	NUM
eurjchem-1000	96	15	mm	mm	NOUN
eurjchem-1000	96	16	x	x	SYM
eurjchem-1000	96	17	2.1	2.1	NUM
eurjchem-1000	96	18	mm	mm	NOUN
eurjchem-1000	96	19	,	,	PUNCT
eurjchem-1000	96	20	5	5	NUM
eurjchem-1000	96	21	μm	μm	NOUN
eurjchem-1000	96	22	)	)	PUNCT
eurjchem-1000	96	23	which	which	PRON
eurjchem-1000	96	24	gave	give	VERB
eurjchem-1000	96	25	a	a	DET
eurjchem-1000	96	26	good	good	ADJ
eurjchem-1000	96	27	peak	peak	NOUN
eurjchem-1000	96	28	shape	shape	NOUN
eurjchem-1000	96	29	and	and	CCONJ
eurjchem-1000	96	30	response	response	NOUN
eurjchem-1000	96	31	even	even	ADV
eurjchem-1000	96	32	at	at	ADP
eurjchem-1000	96	33	lower	low	ADJ
eurjchem-1000	96	34	limit	limit	NOUN
eurjchem-1000	96	35	of	of	ADP
eurjchem-1000	96	36	quantitation	quantitation	NOUN
eurjchem-1000	96	37	level	level	NOUN
eurjchem-1000	96	38	.	.	PUNCT
eurjchem-1000	97	1	a	a	DET
eurjchem-1000	97	2	flow‐rate	flow‐rate	NOUN
eurjchem-1000	97	3	of	of	ADP
eurjchem-1000	97	4	0.5	0.5	NUM
eurjchem-1000	97	5	ml	ml	NOUN
eurjchem-1000	97	6	/	/	SYM
eurjchem-1000	97	7	min	min	NOUN
eurjchem-1000	97	8	produced	produce	VERB
eurjchem-1000	97	9	a	a	DET
eurjchem-1000	97	10	good	good	ADJ
eurjchem-1000	97	11	peak	peak	NOUN
eurjchem-1000	97	12	shape	shape	NOUN
eurjchem-1000	97	13	and	and	CCONJ
eurjchem-1000	97	14	permitted	permit	VERB
eurjchem-1000	97	15	a	a	DET
eurjchem-1000	97	16	runtime	runtime	NOUN
eurjchem-1000	97	17	to	to	ADP
eurjchem-1000	97	18	0.5	0.5	NUM
eurjchem-1000	97	19	min	min	NOUN
eurjchem-1000	97	20	.	.	PROPN
eurjchem-1000	97	21	3.1.3	3.1.3	NUM
eurjchem-1000	97	22	.	.	PUNCT
eurjchem-1000	97	23	plasma	plasma	NOUN
eurjchem-1000	97	24	sample	sample	NOUN
eurjchem-1000	97	25	extraction	extraction	NOUN
eurjchem-1000	97	26	different	different	ADJ
eurjchem-1000	97	27	methods	method	NOUN
eurjchem-1000	97	28	of	of	ADP
eurjchem-1000	97	29	sample	sample	NOUN
eurjchem-1000	97	30	extraction	extraction	NOUN
eurjchem-1000	97	31	including	include	VERB
eurjchem-1000	97	32	protein	protein	NOUN
eurjchem-1000	97	33	precipitation	precipitation	NOUN
eurjchem-1000	97	34	with	with	ADP
eurjchem-1000	97	35	methanol	methanol	NOUN
eurjchem-1000	97	36	or	or	CCONJ
eurjchem-1000	97	37	acetonitrile	acetonitrile	NOUN
eurjchem-1000	97	38	and	and	CCONJ
eurjchem-1000	97	39	liquid‐liquid	liquid‐liquid	ADJ
eurjchem-1000	97	40	extraction	extraction	NOUN
eurjchem-1000	97	41	(	(	PUNCT
eurjchem-1000	97	42	lle	lle	PROPN
eurjchem-1000	97	43	)	)	PUNCT
eurjchem-1000	97	44	with	with	ADP
eurjchem-1000	97	45	different	different	ADJ
eurjchem-1000	97	46	solvents	solvent	NOUN
eurjchem-1000	97	47	commonly	commonly	ADV
eurjchem-1000	97	48	used	use	VERB
eurjchem-1000	97	49	were	be	AUX
eurjchem-1000	97	50	attempted	attempt	VERB
eurjchem-1000	97	51	.	.	PUNCT
eurjchem-1000	98	1	better	well	ADJ
eurjchem-1000	98	2	recoveries	recovery	NOUN
eurjchem-1000	98	3	were	be	AUX
eurjchem-1000	98	4	obtained	obtain	VERB
eurjchem-1000	98	5	with	with	ADP
eurjchem-1000	98	6	lle	lle	NOUN
eurjchem-1000	98	7	using	use	VERB
eurjchem-1000	98	8	tert‐butyl	tert‐butyl	ADP
eurjchem-1000	98	9	methyl	methyl	NOUN
eurjchem-1000	98	10	ether	ether	NOUN
eurjchem-1000	98	11	.	.	PUNCT
eurjchem-1000	99	1	besides	besides	SCONJ
eurjchem-1000	99	2	,	,	PUNCT
eurjchem-1000	99	3	lle	lle	PROPN
eurjchem-1000	99	4	can	can	AUX
eurjchem-1000	99	5	be	be	AUX
eurjchem-1000	99	6	helpful	helpful	ADJ
eurjchem-1000	99	7	in	in	ADP
eurjchem-1000	99	8	producing	produce	VERB
eurjchem-1000	99	9	a	a	DET
eurjchem-1000	99	10	spectroscopically	spectroscopically	ADV
eurjchem-1000	99	11	clean	clean	ADJ
eurjchem-1000	99	12	sample	sample	NOUN
eurjchem-1000	99	13	and	and	CCONJ
eurjchem-1000	99	14	avoiding	avoid	VERB
eurjchem-1000	99	15	the	the	DET
eurjchem-1000	99	16	introduction	introduction	NOUN
eurjchem-1000	99	17	of	of	ADP
eurjchem-1000	99	18	nonvolatile	nonvolatile	ADJ
eurjchem-1000	99	19	materials	material	NOUN
eurjchem-1000	99	20	onto	onto	ADP
eurjchem-1000	99	21	the	the	DET
eurjchem-1000	99	22	column	column	NOUN
eurjchem-1000	99	23	and	and	CCONJ
eurjchem-1000	99	24	ms	ms	NOUN
eurjchem-1000	99	25	system	system	NOUN
eurjchem-1000	99	26	and	and	CCONJ
eurjchem-1000	99	27	also	also	ADV
eurjchem-1000	99	28	minimized	minimize	VERB
eurjchem-1000	99	29	the	the	DET
eurjchem-1000	99	30	experimental	experimental	ADJ
eurjchem-1000	99	31	cost	cost	NOUN
eurjchem-1000	99	32	.	.	PUNCT
eurjchem-1000	100	1	clean	clean	ADJ
eurjchem-1000	100	2	samples	sample	NOUN
eurjchem-1000	100	3	are	be	AUX
eurjchem-1000	100	4	essential	essential	ADJ
eurjchem-1000	100	5	for	for	ADP
eurjchem-1000	100	6	minimizing	minimize	VERB
eurjchem-1000	100	7	ion	ion	NOUN
eurjchem-1000	100	8	suppression	suppression	NOUN
eurjchem-1000	100	9	and	and	CCONJ
eurjchem-1000	100	10	matrix	matrix	NOUN
eurjchem-1000	100	11	effect	effect	NOUN
eurjchem-1000	100	12	in	in	ADP
eurjchem-1000	100	13	lc‐ms	lc‐ms	AUX
eurjchem-1000	100	14	/	/	SYM
eurjchem-1000	100	15	ms	ms	NOUN
eurjchem-1000	100	16	analyses	analysis	NOUN
eurjchem-1000	100	17	.	.	PUNCT
eurjchem-1000	101	1	tert‐butyl	tert‐butyl	PRON
eurjchem-1000	101	2	methyl	methyl	NOUN
eurjchem-1000	101	3	ether	ether	NOUN
eurjchem-1000	101	4	was	be	AUX
eurjchem-1000	101	5	found	find	VERB
eurjchem-1000	101	6	to	to	PART
eurjchem-1000	101	7	be	be	AUX
eurjchem-1000	101	8	optimal	optimal	ADJ
eurjchem-1000	101	9	,	,	PUNCT
eurjchem-1000	101	10	which	which	PRON
eurjchem-1000	101	11	can	can	AUX
eurjchem-1000	101	12	produce	produce	VERB
eurjchem-1000	101	13	a	a	DET
eurjchem-1000	101	14	clean	clean	ADJ
eurjchem-1000	101	15	chromatogram	chromatogram	NOUN
eurjchem-1000	101	16	for	for	ADP
eurjchem-1000	101	17	a	a	DET
eurjchem-1000	101	18	blank	blank	ADJ
eurjchem-1000	101	19	plasma	plasma	NOUN
eurjchem-1000	101	20	sample	sample	NOUN
eurjchem-1000	101	21	and	and	CCONJ
eurjchem-1000	101	22	yield	yield	VERB
eurjchem-1000	101	23	the	the	DET
eurjchem-1000	101	24	highest	high	ADJ
eurjchem-1000	101	25	recovery	recovery	NOUN
eurjchem-1000	101	26	for	for	ADP
eurjchem-1000	101	27	the	the	DET
eurjchem-1000	101	28	drug	drug	NOUN
eurjchem-1000	101	29	from	from	ADP
eurjchem-1000	101	30	the	the	DET
eurjchem-1000	101	31	plasma	plasma	NOUN
eurjchem-1000	101	32	.	.	PUNCT
eurjchem-1000	102	1	3.2	3.2	NUM
eurjchem-1000	102	2	.	.	PUNCT
eurjchem-1000	102	3	method	method	NOUN
eurjchem-1000	102	4	validation	validation	NOUN
eurjchem-1000	102	5	3.2.1	3.2.1	NUM
eurjchem-1000	102	6	.	.	PUNCT
eurjchem-1000	103	1	linearity	linearity	NOUN
eurjchem-1000	103	2	six	six	NUM
eurjchem-1000	103	3	calibration	calibration	NOUN
eurjchem-1000	103	4	curves	curve	NOUN
eurjchem-1000	103	5	each	each	DET
eurjchem-1000	103	6	consisting	consist	VERB
eurjchem-1000	103	7	of	of	ADP
eurjchem-1000	103	8	a	a	DET
eurjchem-1000	103	9	zero	zero	NUM
eurjchem-1000	103	10	,	,	PUNCT
eurjchem-1000	103	11	non‐zero	non‐zero	NUM
eurjchem-1000	103	12	and	and	CCONJ
eurjchem-1000	103	13	calibration	calibration	NOUN
eurjchem-1000	103	14	standards	standard	NOUN
eurjchem-1000	103	15	prepared	prepare	VERB
eurjchem-1000	103	16	in	in	ADP
eurjchem-1000	103	17	human	human	ADJ
eurjchem-1000	103	18	plasma	plasma	NOUN
eurjchem-1000	103	19	were	be	AUX
eurjchem-1000	103	20	chromatographed	chromatographe	VERB
eurjchem-1000	103	21	.	.	PUNCT
eurjchem-1000	104	1	the	the	DET
eurjchem-1000	104	2	concentrations	concentration	NOUN
eurjchem-1000	104	3	of	of	ADP
eurjchem-1000	104	4	calibration	calibration	NOUN
eurjchem-1000	104	5	standards	standard	NOUN
eurjchem-1000	104	6	cover	cover	VERB
eurjchem-1000	104	7	the	the	DET
eurjchem-1000	104	8	range	range	NOUN
eurjchem-1000	104	9	(	(	PUNCT
eurjchem-1000	104	10	5	5	NUM
eurjchem-1000	104	11	‐1500	‐1500	PROPN
eurjchem-1000	104	12	ng	ng	PROPN
eurjchem-1000	104	13	/	/	SYM
eurjchem-1000	104	14	ml	ml	PROPN
eurjchem-1000	104	15	)	)	PUNCT
eurjchem-1000	104	16	,	,	PUNCT
eurjchem-1000	104	17	the	the	DET
eurjchem-1000	104	18	linearity	linearity	NOUN
eurjchem-1000	104	19	was	be	AUX
eurjchem-1000	104	20	evaluated	evaluate	VERB
eurjchem-1000	104	21	by	by	ADP
eurjchem-1000	104	22	calculating	calculate	VERB
eurjchem-1000	104	23	the	the	DET
eurjchem-1000	104	24	linear	linear	ADJ
eurjchem-1000	104	25	regression	regression	NOUN
eurjchem-1000	104	26	(	(	PUNCT
eurjchem-1000	104	27	correlation	correlation	NOUN
eurjchem-1000	104	28	coefficient	coefficient	NOUN
eurjchem-1000	104	29	,	,	PUNCT
eurjchem-1000	104	30	r2	r2	PROPN
eurjchem-1000	104	31	)	)	PUNCT
eurjchem-1000	104	32	,	,	PUNCT
eurjchem-1000	104	33	and	and	CCONJ
eurjchem-1000	104	34	by	by	ADP
eurjchem-1000	104	35	evaluating	evaluate	VERB
eurjchem-1000	104	36	the	the	DET
eurjchem-1000	104	37	back	back	ADV
eurjchem-1000	104	38	calculated	calculate	VERB
eurjchem-1000	104	39	concentrations	concentration	NOUN
eurjchem-1000	104	40	of	of	ADP
eurjchem-1000	104	41	the	the	DET
eurjchem-1000	104	42	calibration	calibration	NOUN
eurjchem-1000	104	43	standards	standard	NOUN
eurjchem-1000	104	44	.	.	PUNCT
eurjchem-1000	105	1	the	the	DET
eurjchem-1000	105	2	lower	low	ADJ
eurjchem-1000	105	3	limit	limit	NOUN
eurjchem-1000	105	4	of	of	ADP
eurjchem-1000	105	5	quantification	quantification	NOUN
eurjchem-1000	105	6	(	(	PUNCT
eurjchem-1000	105	7	lloq	lloq	NOUN
eurjchem-1000	105	8	)	)	PUNCT
eurjchem-1000	105	9	of	of	ADP
eurjchem-1000	105	10	azithromycin	azithromycin	PROPN
eurjchem-1000	105	11	is	be	AUX
eurjchem-1000	105	12	(	(	PUNCT
eurjchem-1000	105	13	5	5	NUM
eurjchem-1000	105	14	ng	ng	PROPN
eurjchem-1000	105	15	/	/	SYM
eurjchem-1000	105	16	ml	ml	NOUN
eurjchem-1000	105	17	)	)	PUNCT
eurjchem-1000	105	18	.	.	PUNCT
eurjchem-1000	106	1	calibration	calibration	NOUN
eurjchem-1000	106	2	curves	curve	NOUN
eurjchem-1000	106	3	are	be	AUX
eurjchem-1000	106	4	found	find	VERB
eurjchem-1000	106	5	to	to	PART
eurjchem-1000	106	6	be	be	AUX
eurjchem-1000	106	7	consistently	consistently	ADV
eurjchem-1000	106	8	accurate	accurate	ADJ
eurjchem-1000	106	9	and	and	CCONJ
eurjchem-1000	106	10	precise	precise	ADJ
eurjchem-1000	106	11	over	over	ADP
eurjchem-1000	106	12	the	the	DET
eurjchem-1000	106	13	calibration	calibration	NOUN
eurjchem-1000	106	14	range	range	NOUN
eurjchem-1000	106	15	of	of	ADP
eurjchem-1000	106	16	5‐1500	5‐1500	NUM
eurjchem-1000	106	17	ng	ng	PROPN
eurjchem-1000	106	18	/	/	SYM
eurjchem-1000	106	19	ml	ml	PROPN
eurjchem-1000	106	20	.	.	PUNCT
eurjchem-1000	107	1	the	the	DET
eurjchem-1000	107	2	mean	mean	ADJ
eurjchem-1000	107	3	correlation	correlation	NOUN
eurjchem-1000	107	4	coefficient	coefficient	NOUN
eurjchem-1000	107	5	(	(	PUNCT
eurjchem-1000	107	6	r2	r2	PROPN
eurjchem-1000	107	7	)	)	PUNCT
eurjchem-1000	107	8	is	be	AUX
eurjchem-1000	107	9	equal	equal	ADJ
eurjchem-1000	107	10	to	to	ADP
eurjchem-1000	107	11	0.999	0.999	NUM
eurjchem-1000	107	12	.	.	PUNCT
eurjchem-1000	108	1	back	back	ADJ
eurjchem-1000	108	2	calculations	calculation	NOUN
eurjchem-1000	108	3	were	be	AUX
eurjchem-1000	108	4	made	make	VERB
eurjchem-1000	108	5	from	from	ADP
eurjchem-1000	108	6	the	the	DET
eurjchem-1000	108	7	calibration	calibration	NOUN
eurjchem-1000	108	8	curves	curve	NOUN
eurjchem-1000	108	9	to	to	PART
eurjchem-1000	108	10	determine	determine	VERB
eurjchem-1000	108	11	drug	drug	NOUN
eurjchem-1000	108	12	concentrations	concentration	NOUN
eurjchem-1000	108	13	of	of	ADP
eurjchem-1000	108	14	each	each	DET
eurjchem-1000	108	15	calibration	calibration	NOUN
eurjchem-1000	108	16	standard	standard	NOUN
eurjchem-1000	108	17	.	.	PUNCT
eurjchem-1000	109	1	data	datum	NOUN
eurjchem-1000	109	2	are	be	AUX
eurjchem-1000	109	3	presented	present	VERB
eurjchem-1000	109	4	in	in	ADP
eurjchem-1000	109	5	table	table	NOUN
eurjchem-1000	109	6	2	2	NUM
eurjchem-1000	109	7	.	.	PUNCT
eurjchem-1000	110	1	a	a	DET
eurjchem-1000	110	2	typical	typical	ADJ
eurjchem-1000	110	3	calibration	calibration	NOUN
eurjchem-1000	110	4	curve	curve	NOUN
eurjchem-1000	110	5	is	be	AUX
eurjchem-1000	110	6	presented	present	VERB
eurjchem-1000	110	7	in	in	ADP
eurjchem-1000	110	8	figure	figure	NOUN
eurjchem-1000	110	9	4	4	NUM
eurjchem-1000	110	10	.	.	PUNCT
eurjchem-1000	111	1	3.2.2	3.2.2	NUM
eurjchem-1000	111	2	.	.	PUNCT
eurjchem-1000	112	1	selectivity	selectivity	VERB
eurjchem-1000	112	2	the	the	DET
eurjchem-1000	112	3	selectivity	selectivity	NOUN
eurjchem-1000	112	4	of	of	ADP
eurjchem-1000	112	5	the	the	DET
eurjchem-1000	112	6	method	method	NOUN
eurjchem-1000	112	7	was	be	AUX
eurjchem-1000	112	8	examined	examine	VERB
eurjchem-1000	112	9	by	by	ADP
eurjchem-1000	112	10	analyzing	analyze	VERB
eurjchem-1000	112	11	a	a	DET
eurjchem-1000	112	12	blank	blank	ADJ
eurjchem-1000	112	13	human	human	ADJ
eurjchem-1000	112	14	plasma	plasma	NOUN
eurjchem-1000	112	15	extract	extract	NOUN
eurjchem-1000	112	16	and	and	CCONJ
eurjchem-1000	112	17	a	a	DET
eurjchem-1000	112	18	blank	blank	ADJ
eurjchem-1000	112	19	plasma	plasma	NOUN
eurjchem-1000	112	20	sample	sample	NOUN
eurjchem-1000	112	21	spiked	spike	VERB
eurjchem-1000	112	22	with	with	ADP
eurjchem-1000	112	23	is	be	AUX
eurjchem-1000	112	24	only	only	ADV
eurjchem-1000	112	25	(	(	PUNCT
eurjchem-1000	112	26	figure	figure	NOUN
eurjchem-1000	112	27	5	5	NUM
eurjchem-1000	112	28	)	)	PUNCT
eurjchem-1000	112	29	.	.	PUNCT
eurjchem-1000	113	1	as	as	SCONJ
eurjchem-1000	113	2	shown	show	VERB
eurjchem-1000	113	3	in	in	ADP
eurjchem-1000	113	4	this	this	DET
eurjchem-1000	113	5	figure	figure	NOUN
eurjchem-1000	113	6	,	,	PUNCT
eurjchem-1000	113	7	no	no	DET
eurjchem-1000	113	8	significant	significant	ADJ
eurjchem-1000	113	9	interferences	interference	NOUN
eurjchem-1000	113	10	were	be	AUX
eurjchem-1000	113	11	observed	observe	VERB
eurjchem-1000	113	12	in	in	ADP
eurjchem-1000	113	13	the	the	DET
eurjchem-1000	113	14	lots	lot	NOUN
eurjchem-1000	113	15	of	of	ADP
eurjchem-1000	113	16	human	human	ADJ
eurjchem-1000	113	17	plasma	plasma	NOUN
eurjchem-1000	113	18	used	use	VERB
eurjchem-1000	113	19	for	for	ADP
eurjchem-1000	113	20	the	the	DET
eurjchem-1000	113	21	preparation	preparation	NOUN
eurjchem-1000	113	22	of	of	ADP
eurjchem-1000	113	23	calibration	calibration	NOUN
eurjchem-1000	113	24	standards	standard	NOUN
eurjchem-1000	113	25	and	and	CCONJ
eurjchem-1000	113	26	quality	quality	NOUN
eurjchem-1000	113	27	control	control	NOUN
eurjchem-1000	113	28	samples	sample	NOUN
eurjchem-1000	113	29	.	.	PUNCT
eurjchem-1000	114	1	3.2.3	3.2.3	X
eurjchem-1000	114	2	.	.	PUNCT
eurjchem-1000	114	3	lloq	lloq	VERB
eurjchem-1000	114	4	the	the	DET
eurjchem-1000	114	5	lowest	low	ADJ
eurjchem-1000	114	6	limit	limit	NOUN
eurjchem-1000	114	7	of	of	ADP
eurjchem-1000	114	8	reliable	reliable	ADJ
eurjchem-1000	114	9	quantification	quantification	NOUN
eurjchem-1000	114	10	for	for	ADP
eurjchem-1000	114	11	the	the	DET
eurjchem-1000	114	12	drug	drug	NOUN
eurjchem-1000	114	13	was	be	AUX
eurjchem-1000	114	14	set	set	VERB
eurjchem-1000	114	15	at	at	ADP
eurjchem-1000	114	16	the	the	DET
eurjchem-1000	114	17	concentration	concentration	NOUN
eurjchem-1000	114	18	of	of	ADP
eurjchem-1000	114	19	the	the	DET
eurjchem-1000	114	20	lloq	lloq	NOUN
eurjchem-1000	114	21	which	which	PRON
eurjchem-1000	114	22	is	be	AUX
eurjchem-1000	114	23	the	the	DET
eurjchem-1000	114	24	lowest	low	ADJ
eurjchem-1000	114	25	quality	quality	NOUN
eurjchem-1000	114	26	control	control	NOUN
eurjchem-1000	114	27	level	level	NOUN
eurjchem-1000	114	28	with	with	ADP
eurjchem-1000	114	29	a	a	DET
eurjchem-1000	114	30	coefficient	coefficient	NOUN
eurjchem-1000	114	31	of	of	ADP
eurjchem-1000	114	32	variation	variation	NOUN
eurjchem-1000	114	33	less	less	ADJ
eurjchem-1000	114	34	than	than	ADP
eurjchem-1000	114	35	20	20	NUM
eurjchem-1000	114	36	%	%	NOUN
eurjchem-1000	114	37	.	.	PUNCT
eurjchem-1000	115	1	lloq	lloq	PROPN
eurjchem-1000	115	2	is	be	AUX
eurjchem-1000	115	3	5	5	NUM
eurjchem-1000	115	4	ng	ng	NOUN
eurjchem-1000	115	5	/	/	SYM
eurjchem-1000	115	6	ml	ml	NOUN
eurjchem-1000	115	7	with	with	ADP
eurjchem-1000	115	8	a	a	DET
eurjchem-1000	115	9	signal	signal	NOUN
eurjchem-1000	115	10	to	to	PART
eurjchem-1000	115	11	noise	noise	VERB
eurjchem-1000	115	12	ratio	ratio	NOUN
eurjchem-1000	115	13	of	of	ADP
eurjchem-1000	115	14	6.1	6.1	NUM
eurjchem-1000	115	15	.	.	PUNCT
eurjchem-1000	116	1	244	244	NUM
eurjchem-1000	116	2	younes	younes	PROPN
eurjchem-1000	116	3	and	and	CCONJ
eurjchem-1000	116	4	el‐kady	el‐kady	PROPN
eurjchem-1000	116	5	/	/	SYM
eurjchem-1000	116	6	european	european	PROPN
eurjchem-1000	116	7	journal	journal	PROPN
eurjchem-1000	116	8	of	of	ADP
eurjchem-1000	116	9	chemistry	chemistry	NOUN
eurjchem-1000	116	10	5	5	NUM
eurjchem-1000	116	11	(	(	PUNCT
eurjchem-1000	116	12	2	2	NUM
eurjchem-1000	116	13	)	)	PUNCT
eurjchem-1000	116	14	(	(	PUNCT
eurjchem-1000	116	15	2014	2014	NUM
eurjchem-1000	116	16	)	)	PUNCT
eurjchem-1000	116	17	241‐246	241‐246	NUM
eurjchem-1000	116	18	table	table	NOUN
eurjchem-1000	116	19	2	2	NUM
eurjchem-1000	116	20	.	.	PUNCT
eurjchem-1000	116	21	back‐calculated	back‐calculated	ADJ
eurjchem-1000	116	22	standards	standard	NOUN
eurjchem-1000	116	23	from	from	ADP
eurjchem-1000	116	24	each	each	DET
eurjchem-1000	116	25	calibration	calibration	NOUN
eurjchem-1000	116	26	curve	curve	NOUN
eurjchem-1000	116	27	.	.	PUNCT
eurjchem-1000	117	1	calibration	calibration	NOUN
eurjchem-1000	117	2	no	no	DET
eurjchem-1000	117	3	nominal	nominal	ADJ
eurjchem-1000	117	4	concentrations	concentration	NOUN
eurjchem-1000	117	5	(	(	PUNCT
eurjchem-1000	117	6	ng	ng	NOUN
eurjchem-1000	117	7	/	/	SYM
eurjchem-1000	117	8	ml	ml	NOUN
eurjchem-1000	117	9	)	)	PUNCT
eurjchem-1000	117	10	5	5	NUM
eurjchem-1000	117	11	25	25	NUM
eurjchem-1000	117	12	50	50	NUM
eurjchem-1000	117	13	100	100	NUM
eurjchem-1000	117	14	250	250	NUM
eurjchem-1000	117	15	500	500	NUM
eurjchem-1000	117	16	1000	1000	NUM
eurjchem-1000	117	17	1500	1500	NUM
eurjchem-1000	117	18	1	1	NUM
eurjchem-1000	117	19	5.414	5.414	NUM
eurjchem-1000	117	20	24.873	24.873	NUM
eurjchem-1000	117	21	49.112	49.112	NUM
eurjchem-1000	117	22	111.359	111.359	NUM
eurjchem-1000	117	23	256.809	256.809	NUM
eurjchem-1000	117	24	513.472	513.472	NUM
eurjchem-1000	117	25	1004.263	1004.263	NUM
eurjchem-1000	117	26	1558.137	1558.137	NUM
eurjchem-1000	117	27	2	2	NUM
eurjchem-1000	117	28	5.165	5.165	NUM
eurjchem-1000	117	29	25.455	25.455	NUM
eurjchem-1000	117	30	45.562	45.562	NUM
eurjchem-1000	117	31	111.180	111.180	NUM
eurjchem-1000	117	32	253.650	253.650	NUM
eurjchem-1000	117	33	524.688	524.688	NUM
eurjchem-1000	117	34	979.228	979.228	NUM
eurjchem-1000	117	35	1513.784	1513.784	NUM
eurjchem-1000	117	36	3	3	NUM
eurjchem-1000	117	37	5.240	5.240	NUM
eurjchem-1000	117	38	24.936	24.936	NUM
eurjchem-1000	117	39	42.811	42.811	NUM
eurjchem-1000	117	40	110.972	110.972	NUM
eurjchem-1000	117	41	246.615	246.615	NUM
eurjchem-1000	117	42	515.740	515.740	NUM
eurjchem-1000	117	43	1004.699	1004.699	NUM
eurjchem-1000	117	44	1406.883	1406.883	NUM
eurjchem-1000	117	45	4	4	NUM
eurjchem-1000	117	46	6.054	6.054	NUM
eurjchem-1000	117	47	22.758	22.758	NUM
eurjchem-1000	117	48	42.811	42.811	NUM
eurjchem-1000	117	49	104.843	104.843	NUM
eurjchem-1000	117	50	240.341	240.341	NUM
eurjchem-1000	117	51	507.540	507.540	NUM
eurjchem-1000	117	52	981.047	981.047	NUM
eurjchem-1000	117	53	1513.023	1513.023	PROPN
eurjchem-1000	117	54	5	5	NUM
eurjchem-1000	117	55	5.868	5.868	NUM
eurjchem-1000	117	56	24.936	24.936	NUM
eurjchem-1000	117	57	42.811	42.811	NUM
eurjchem-1000	117	58	110.999	110.999	NUM
eurjchem-1000	117	59	246.615	246.615	NUM
eurjchem-1000	117	60	515.740	515.740	NUM
eurjchem-1000	117	61	1004.699	1004.699	NUM
eurjchem-1000	117	62	1554.451	1554.451	NUM
eurjchem-1000	117	63	6	6	NUM
eurjchem-1000	117	64	5.266	5.266	NUM
eurjchem-1000	117	65	22.000	22.000	NUM
eurjchem-1000	117	66	43.350	43.350	NUM
eurjchem-1000	117	67	134.416	134.416	NUM
eurjchem-1000	117	68	248.320	248.320	NUM
eurjchem-1000	117	69	496.705	496.705	NUM
eurjchem-1000	117	70	1004.699	1004.699	NUM
eurjchem-1000	117	71	1538.047	1538.047	NUM
eurjchem-1000	117	72	n	n	NUM
eurjchem-1000	117	73	6	6	NUM
eurjchem-1000	117	74	6	6	NUM
eurjchem-1000	117	75	6	6	NUM
eurjchem-1000	117	76	6	6	NUM
eurjchem-1000	117	77	6	6	NUM
eurjchem-1000	117	78	6	6	NUM
eurjchem-1000	117	79	6	6	NUM
eurjchem-1000	117	80	6	6	NUM
eurjchem-1000	117	81	mean	mean	NOUN
eurjchem-1000	117	82	5.501	5.501	NUM
eurjchem-1000	117	83	24.160	24.160	NUM
eurjchem-1000	117	84	44.410	44.410	NUM
eurjchem-1000	117	85	113.961	113.961	NUM
eurjchem-1000	117	86	248.725	248.725	NUM
eurjchem-1000	117	87	512.314	512.314	NUM
eurjchem-1000	117	88	996.439	996.439	NUM
eurjchem-1000	117	89	1514.054	1514.054	NUM
eurjchem-1000	117	90	sd	sd	PROPN
eurjchem-1000	117	91	(	(	PUNCT
eurjchem-1000	117	92	±	±	NOUN
eurjchem-1000	117	93	)	)	PUNCT
eurjchem-1000	117	94	0.370	0.370	NUM
eurjchem-1000	117	95	1.416	1.416	NUM
eurjchem-1000	117	96	2.539	2.539	NUM
eurjchem-1000	117	97	10.332	10.332	NUM
eurjchem-1000	117	98	5.813	5.813	NUM
eurjchem-1000	117	99	9.427	9.427	NUM
eurjchem-1000	117	100	12.642	12.642	NUM
eurjchem-1000	117	101	55.92411	55.92411	NUM
eurjchem-1000	117	102	cv	cv	NOUN
eurjchem-1000	117	103	(	(	PUNCT
eurjchem-1000	117	104	%	%	NOUN
eurjchem-1000	117	105	)	)	PUNCT
eurjchem-1000	117	106	6.723	6.723	NUM
eurjchem-1000	117	107	5.860	5.860	NUM
eurjchem-1000	117	108	5.717	5.717	NUM
eurjchem-1000	117	109	9.066	9.066	NUM
eurjchem-1000	117	110	2.337	2.337	NUM
eurjchem-1000	117	111	1.840	1.840	NUM
eurjchem-1000	117	112	1.269	1.269	NUM
eurjchem-1000	117	113	3.693667	3.693667	NUM
eurjchem-1000	117	114	%	%	NOUN
eurjchem-1000	117	115	nominal	nominal	ADJ
eurjchem-1000	117	116	110.022	110.022	NUM
eurjchem-1000	117	117	96.640	96.640	NUM
eurjchem-1000	117	118	88.819	88.819	NUM
eurjchem-1000	117	119	113.961	113.961	NUM
eurjchem-1000	117	120	99.490	99.490	NUM
eurjchem-1000	117	121	102.463	102.463	NUM
eurjchem-1000	117	122	99.644	99.644	NUM
eurjchem-1000	117	123	100.9369	100.9369	NUM
eurjchem-1000	117	124	table	table	NOUN
eurjchem-1000	117	125	3	3	NUM
eurjchem-1000	117	126	.	.	NOUN
eurjchem-1000	117	127	intra‐day	intra‐day	PROPN
eurjchem-1000	117	128	accuracy	accuracy	NOUN
eurjchem-1000	117	129	and	and	CCONJ
eurjchem-1000	117	130	precision	precision	NOUN
eurjchem-1000	117	131	.	.	PUNCT
eurjchem-1000	118	1	run	run	NOUN
eurjchem-1000	118	2	number	number	NOUN
eurjchem-1000	118	3	qcl	qcl	PROPN
eurjchem-1000	118	4	10	10	NUM
eurjchem-1000	118	5	ng	ng	NOUN
eurjchem-1000	118	6	/	/	SYM
eurjchem-1000	118	7	ml	ml	AUX
eurjchem-1000	118	8	qcm	qcm	VERB
eurjchem-1000	118	9	400	400	NUM
eurjchem-1000	118	10	ng	ng	NOUN
eurjchem-1000	118	11	/	/	SYM
eurjchem-1000	118	12	ml	ml	NOUN
eurjchem-1000	118	13	qch	qch	NOUN
eurjchem-1000	118	14	1200	1200	NUM
eurjchem-1000	118	15	ng	ng	PROPN
eurjchem-1000	118	16	/	/	SYM
eurjchem-1000	118	17	ml	ml	NOUN
eurjchem-1000	118	18	conc	conc	VERB
eurjchem-1000	118	19	.	.	PUNCT
eurjchem-1000	119	1	found	find	VERB
eurjchem-1000	119	2	(	(	PUNCT
eurjchem-1000	119	3	ng	ng	NOUN
eurjchem-1000	119	4	/	/	SYM
eurjchem-1000	119	5	ml	ml	NOUN
eurjchem-1000	119	6	)	)	PUNCT
eurjchem-1000	119	7	%	%	NOUN
eurjchem-1000	119	8	nominal	nominal	ADJ
eurjchem-1000	119	9	conc	conc	NOUN
eurjchem-1000	119	10	.	.	PUNCT
eurjchem-1000	120	1	conc	conc	VERB
eurjchem-1000	120	2	.	.	PUNCT
eurjchem-1000	121	1	found	find	VERB
eurjchem-1000	121	2	(	(	PUNCT
eurjchem-1000	121	3	ng	ng	NOUN
eurjchem-1000	121	4	/	/	SYM
eurjchem-1000	121	5	ml	ml	NOUN
eurjchem-1000	121	6	)	)	PUNCT
eurjchem-1000	121	7	%	%	NOUN
eurjchem-1000	121	8	nominal	nominal	ADJ
eurjchem-1000	121	9	conc	conc	NOUN
eurjchem-1000	121	10	.	.	PUNCT
eurjchem-1000	122	1	conc	conc	VERB
eurjchem-1000	122	2	.	.	PUNCT
eurjchem-1000	123	1	found	find	VERB
eurjchem-1000	123	2	(	(	PUNCT
eurjchem-1000	123	3	ng	ng	NOUN
eurjchem-1000	123	4	/	/	SYM
eurjchem-1000	123	5	ml	ml	NOUN
eurjchem-1000	123	6	)	)	PUNCT
eurjchem-1000	123	7	%	%	NOUN
eurjchem-1000	123	8	nominal	nominal	ADJ
eurjchem-1000	123	9	conc	conc	NOUN
eurjchem-1000	123	10	.	.	PUNCT
eurjchem-1000	124	1	1	1	NUM
eurjchem-1000	124	2	11.23	11.23	NUM
eurjchem-1000	124	3	112.3	112.3	NUM
eurjchem-1000	124	4	384	384	NUM
eurjchem-1000	124	5	96.00	96.00	NUM
eurjchem-1000	124	6	1202	1202	NUM
eurjchem-1000	124	7	100.17	100.17	NUM
eurjchem-1000	124	8	2	2	NUM
eurjchem-1000	124	9	10.24	10.24	NUM
eurjchem-1000	124	10	102.36	102.36	NUM
eurjchem-1000	124	11	399	399	NUM
eurjchem-1000	124	12	99.75	99.75	NUM
eurjchem-1000	124	13	1125	1125	NUM
eurjchem-1000	124	14	93.75	93.75	NUM
eurjchem-1000	124	15	3	3	NUM
eurjchem-1000	124	16	9.63	9.63	NUM
eurjchem-1000	124	17	96.32	96.32	NUM
eurjchem-1000	124	18	374	374	NUM
eurjchem-1000	124	19	93.50	93.50	NUM
eurjchem-1000	124	20	1136	1136	NUM
eurjchem-1000	124	21	94.67	94.67	NUM
eurjchem-1000	124	22	4	4	NUM
eurjchem-1000	124	23	9.32	9.32	NUM
eurjchem-1000	124	24	93.21	93.21	NUM
eurjchem-1000	124	25	386	386	NUM
eurjchem-1000	124	26	96.50	96.50	NUM
eurjchem-1000	124	27	1189	1189	NUM
eurjchem-1000	124	28	99.08	99.08	NUM
eurjchem-1000	124	29	5	5	NUM
eurjchem-1000	124	30	9.75	9.75	NUM
eurjchem-1000	124	31	97.45	97.45	NUM
eurjchem-1000	124	32	401	401	NUM
eurjchem-1000	124	33	100.25	100.25	NUM
eurjchem-1000	124	34	1187	1187	NUM
eurjchem-1000	124	35	98.92	98.92	NUM
eurjchem-1000	124	36	6	6	NUM
eurjchem-1000	124	37	8.52	8.52	NUM
eurjchem-1000	124	38	85.21	85.21	NUM
eurjchem-1000	124	39	422	422	NUM
eurjchem-1000	124	40	105.50	105.50	NUM
eurjchem-1000	124	41	1120	1120	NUM
eurjchem-1000	124	42	93.33	93.33	NUM
eurjchem-1000	124	43	n	n	SYM
eurjchem-1000	124	44	6	6	NUM
eurjchem-1000	124	45	6	6	NUM
eurjchem-1000	124	46	6	6	NUM
eurjchem-1000	124	47	6	6	NUM
eurjchem-1000	124	48	6	6	NUM
eurjchem-1000	124	49	6	6	NUM
eurjchem-1000	124	50	mean	mean	NOUN
eurjchem-1000	124	51	9.78	9.78	NUM
eurjchem-1000	124	52	97.81	97.81	NUM
eurjchem-1000	124	53	394.33	394.33	NUM
eurjchem-1000	124	54	98.58	98.58	NUM
eurjchem-1000	124	55	1159.83	1159.83	NUM
eurjchem-1000	124	56	96.65	96.65	NUM
eurjchem-1000	124	57	sd	sd	ADP
eurjchem-1000	124	58	(	(	PUNCT
eurjchem-1000	124	59	±	±	PROPN
eurjchem-1000	124	60	)	)	PUNCT
eurjchem-1000	124	61	0.91	0.91	NUM
eurjchem-1000	124	62	16.86	16.86	NUM
eurjchem-1000	124	63	36.70	36.70	NUM
eurjchem-1000	124	64	cv	cv	PROPN
eurjchem-1000	124	65	(	(	PUNCT
eurjchem-1000	124	66	%	%	NOUN
eurjchem-1000	124	67	)	)	PUNCT
eurjchem-1000	124	68	9.29	9.29	NUM
eurjchem-1000	124	69	4.28	4.28	NUM
eurjchem-1000	124	70	3.16	3.16	NUM
eurjchem-1000	124	71	figure	figure	NOUN
eurjchem-1000	124	72	4	4	NUM
eurjchem-1000	124	73	.	.	PUNCT
eurjchem-1000	124	74	standard	standard	ADJ
eurjchem-1000	124	75	calibration	calibration	NOUN
eurjchem-1000	124	76	curve	curve	NOUN
eurjchem-1000	124	77	of	of	ADP
eurjchem-1000	124	78	azithromycin	azithromycin	PROPN
eurjchem-1000	124	79	in	in	ADP
eurjchem-1000	124	80	human	human	ADJ
eurjchem-1000	124	81	plasma	plasma	NOUN
eurjchem-1000	124	82	.	.	PUNCT
eurjchem-1000	125	1	figure	figure	NOUN
eurjchem-1000	125	2	5	5	NUM
eurjchem-1000	125	3	.	.	PUNCT
eurjchem-1000	125	4	mass	mass	PROPN
eurjchem-1000	125	5	spectrum	spectrum	NOUN
eurjchem-1000	125	6	of	of	ADP
eurjchem-1000	125	7	blank	blank	ADJ
eurjchem-1000	125	8	plasma	plasma	NOUN
eurjchem-1000	125	9	compared	compare	VERB
eurjchem-1000	125	10	to	to	ADP
eurjchem-1000	125	11	that	that	PRON
eurjchem-1000	125	12	containing	contain	VERB
eurjchem-1000	125	13	only	only	ADV
eurjchem-1000	125	14	is	be	AUX
eurjchem-1000	125	15	.	.	PUNCT
eurjchem-1000	126	1	3.2.4	3.2.4	NUM
eurjchem-1000	126	2	.	.	PUNCT
eurjchem-1000	126	3	accuracy	accuracy	NOUN
eurjchem-1000	126	4	and	and	CCONJ
eurjchem-1000	126	5	precision	precision	NOUN
eurjchem-1000	126	6	3.2.4.1	3.2.4.1	NUM
eurjchem-1000	126	7	.	.	PUNCT
eurjchem-1000	126	8	intra‐day	intra‐day	PROPN
eurjchem-1000	126	9	accuracy	accuracy	NOUN
eurjchem-1000	126	10	and	and	CCONJ
eurjchem-1000	126	11	precision	precision	NOUN
eurjchem-1000	126	12	the	the	DET
eurjchem-1000	126	13	intra‐day	intra‐day	NOUN
eurjchem-1000	126	14	accuracy	accuracy	NOUN
eurjchem-1000	126	15	and	and	CCONJ
eurjchem-1000	126	16	precision	precision	NOUN
eurjchem-1000	126	17	evaluations	evaluation	NOUN
eurjchem-1000	126	18	were	be	AUX
eurjchem-1000	126	19	assessed	assess	VERB
eurjchem-1000	126	20	by	by	ADP
eurjchem-1000	126	21	repeated	repeat	VERB
eurjchem-1000	126	22	analysis	analysis	NOUN
eurjchem-1000	126	23	of	of	ADP
eurjchem-1000	126	24	human	human	ADJ
eurjchem-1000	126	25	plasma	plasma	NOUN
eurjchem-1000	126	26	samples	sample	NOUN
eurjchem-1000	126	27	containing	contain	VERB
eurjchem-1000	126	28	different	different	ADJ
eurjchem-1000	126	29	concentrations	concentration	NOUN
eurjchem-1000	126	30	of	of	ADP
eurjchem-1000	126	31	azithromycin	azithromycin	NOUN
eurjchem-1000	126	32	on	on	ADP
eurjchem-1000	126	33	separate	separate	ADJ
eurjchem-1000	126	34	occasions	occasion	NOUN
eurjchem-1000	126	35	,	,	PUNCT
eurjchem-1000	126	36	same	same	ADJ
eurjchem-1000	126	37	day	day	NOUN
eurjchem-1000	126	38	.	.	PUNCT
eurjchem-1000	127	1	a	a	DET
eurjchem-1000	127	2	single	single	ADJ
eurjchem-1000	127	3	run	run	NOUN
eurjchem-1000	127	4	consisted	consist	VERB
eurjchem-1000	127	5	of	of	ADP
eurjchem-1000	127	6	a	a	DET
eurjchem-1000	127	7	calibration	calibration	NOUN
eurjchem-1000	127	8	curve	curve	NOUN
eurjchem-1000	127	9	plus	plus	CCONJ
eurjchem-1000	127	10	6	6	NUM
eurjchem-1000	127	11	runs	run	NOUN
eurjchem-1000	127	12	of	of	ADP
eurjchem-1000	127	13	low	low	ADJ
eurjchem-1000	127	14	(	(	PUNCT
eurjchem-1000	127	15	qcl	qcl	NOUN
eurjchem-1000	127	16	)	)	PUNCT
eurjchem-1000	127	17	,	,	PUNCT
eurjchem-1000	127	18	medium	medium	NOUN
eurjchem-1000	127	19	(	(	PUNCT
eurjchem-1000	127	20	qcm	qcm	NOUN
eurjchem-1000	127	21	)	)	PUNCT
eurjchem-1000	127	22	and	and	CCONJ
eurjchem-1000	127	23	high	high	ADJ
eurjchem-1000	127	24	(	(	PUNCT
eurjchem-1000	127	25	qch	qch	NOUN
eurjchem-1000	127	26	)	)	PUNCT
eurjchem-1000	127	27	quality	quality	NOUN
eurjchem-1000	127	28	control	control	NOUN
eurjchem-1000	127	29	samples	sample	NOUN
eurjchem-1000	127	30	,	,	PUNCT
eurjchem-1000	127	31	the	the	DET
eurjchem-1000	127	32	intra‐day	intra‐day	NOUN
eurjchem-1000	127	33	coefficients	coefficient	NOUN
eurjchem-1000	127	34	of	of	ADP
eurjchem-1000	127	35	variation	variation	NOUN
eurjchem-1000	127	36	ranged	range	VERB
eurjchem-1000	127	37	between	between	ADP
eurjchem-1000	127	38	9.29	9.29	NUM
eurjchem-1000	127	39	,	,	PUNCT
eurjchem-1000	127	40	4.28	4.28	NUM
eurjchem-1000	127	41	and	and	CCONJ
eurjchem-1000	127	42	3.16	3.16	NUM
eurjchem-1000	127	43	%	%	NOUN
eurjchem-1000	127	44	.	.	PUNCT
eurjchem-1000	128	1	the	the	DET
eurjchem-1000	128	2	intra‐day	intra‐day	NOUN
eurjchem-1000	128	3	percentages	percentage	NOUN
eurjchem-1000	128	4	of	of	ADP
eurjchem-1000	128	5	nominal	nominal	ADJ
eurjchem-1000	128	6	concentration	concentration	NOUN
eurjchem-1000	128	7	ranged	range	VERB
eurjchem-1000	128	8	between	between	ADP
eurjchem-1000	128	9	97.81	97.81	NUM
eurjchem-1000	128	10	,	,	PUNCT
eurjchem-1000	128	11	98.58	98.58	NUM
eurjchem-1000	128	12	and	and	CCONJ
eurjchem-1000	128	13	96.65	96.65	NUM
eurjchem-1000	128	14	%	%	NOUN
eurjchem-1000	128	15	.	.	PUNCT
eurjchem-1000	129	1	results	result	NOUN
eurjchem-1000	129	2	are	be	AUX
eurjchem-1000	129	3	presented	present	VERB
eurjchem-1000	129	4	in	in	ADP
eurjchem-1000	129	5	table	table	NOUN
eurjchem-1000	129	6	3	3	NUM
eurjchem-1000	129	7	.	.	X
eurjchem-1000	130	1	3.2.4.2	3.2.4.2	NUM
eurjchem-1000	130	2	.	.	PUNCT
eurjchem-1000	131	1	inter‐day	inter‐day	NOUN
eurjchem-1000	131	2	accuracy	accuracy	NOUN
eurjchem-1000	131	3	and	and	CCONJ
eurjchem-1000	131	4	precision	precision	NOUN
eurjchem-1000	131	5	inter‐day	inter‐day	NOUN
eurjchem-1000	131	6	accuracy	accuracy	NOUN
eurjchem-1000	131	7	and	and	CCONJ
eurjchem-1000	131	8	precision	precision	NOUN
eurjchem-1000	131	9	evaluations	evaluation	NOUN
eurjchem-1000	131	10	were	be	AUX
eurjchem-1000	131	11	performed	perform	VERB
eurjchem-1000	131	12	by	by	ADP
eurjchem-1000	131	13	analyzing	analyze	VERB
eurjchem-1000	131	14	three	three	NUM
eurjchem-1000	131	15	sets	set	NOUN
eurjchem-1000	131	16	of	of	ADP
eurjchem-1000	131	17	qcl	qcl	NOUN
eurjchem-1000	131	18	,	,	PUNCT
eurjchem-1000	131	19	qcm	qcm	NOUN
eurjchem-1000	131	20	and	and	CCONJ
eurjchem-1000	131	21	qch	qch	NOUN
eurjchem-1000	131	22	quality	quality	NOUN
eurjchem-1000	131	23	control	control	NOUN
eurjchem-1000	131	24	samples	sample	NOUN
eurjchem-1000	131	25	of	of	ADP
eurjchem-1000	131	26	azithromycin	azithromycin	NOUN
eurjchem-1000	131	27	in	in	ADP
eurjchem-1000	131	28	human	human	ADJ
eurjchem-1000	131	29	plasma	plasma	NOUN
eurjchem-1000	131	30	.	.	PUNCT
eurjchem-1000	132	1	one	one	NUM
eurjchem-1000	132	2	set	set	NOUN
eurjchem-1000	132	3	was	be	AUX
eurjchem-1000	132	4	extracted	extract	VERB
eurjchem-1000	132	5	and	and	CCONJ
eurjchem-1000	132	6	analyzed	analyze	VERB
eurjchem-1000	132	7	on	on	ADP
eurjchem-1000	132	8	one	one	NUM
eurjchem-1000	132	9	day	day	NOUN
eurjchem-1000	132	10	(	(	PUNCT
eurjchem-1000	132	11	day	day	NOUN
eurjchem-1000	132	12	i	i	NOUN
eurjchem-1000	132	13	)	)	PUNCT
eurjchem-1000	132	14	.	.	PUNCT
eurjchem-1000	133	1	the	the	DET
eurjchem-1000	133	2	other	other	ADJ
eurjchem-1000	133	3	two	two	NUM
eurjchem-1000	133	4	sets	set	NOUN
eurjchem-1000	133	5	were	be	AUX
eurjchem-1000	133	6	kept	keep	VERB
eurjchem-1000	133	7	frozen	freeze	VERB
eurjchem-1000	133	8	,	,	PUNCT
eurjchem-1000	133	9	thawed	thaw	VERB
eurjchem-1000	133	10	,	,	PUNCT
eurjchem-1000	133	11	extracted	extract	VERB
eurjchem-1000	133	12	and	and	CCONJ
eurjchem-1000	133	13	analysed	analyse	VERB
eurjchem-1000	133	14	on	on	ADP
eurjchem-1000	133	15	a	a	DET
eurjchem-1000	133	16	next	next	ADJ
eurjchem-1000	133	17	day	day	NOUN
eurjchem-1000	133	18	(	(	PUNCT
eurjchem-1000	133	19	day	day	PROPN
eurjchem-1000	133	20	ii	ii	PROPN
eurjchem-1000	133	21	)	)	PUNCT
eurjchem-1000	133	22	for	for	ADP
eurjchem-1000	133	23	the	the	DET
eurjchem-1000	133	24	second	second	ADJ
eurjchem-1000	133	25	set	set	NOUN
eurjchem-1000	133	26	,	,	PUNCT
eurjchem-1000	133	27	and	and	CCONJ
eurjchem-1000	133	28	third	third	ADJ
eurjchem-1000	133	29	day	day	NOUN
eurjchem-1000	133	30	(	(	PUNCT
eurjchem-1000	133	31	day	day	NOUN
eurjchem-1000	133	32	iii	iii	NOUN
eurjchem-1000	133	33	)	)	PUNCT
eurjchem-1000	133	34	for	for	ADP
eurjchem-1000	133	35	the	the	DET
eurjchem-1000	133	36	last	last	ADJ
eurjchem-1000	133	37	set	set	NOUN
eurjchem-1000	133	38	.	.	PUNCT
eurjchem-1000	134	1	the	the	DET
eurjchem-1000	134	2	inter‐day	inter‐day	NOUN
eurjchem-1000	134	3	coefficients	coefficient	NOUN
eurjchem-1000	134	4	of	of	ADP
eurjchem-1000	134	5	variation	variation	NOUN
eurjchem-1000	134	6	ranged	range	VERB
eurjchem-1000	134	7	between	between	ADP
eurjchem-1000	134	8	14.50	14.50	NUM
eurjchem-1000	134	9	,	,	PUNCT
eurjchem-1000	134	10	4.70	4.70	NUM
eurjchem-1000	134	11	and	and	CCONJ
eurjchem-1000	134	12	3.40	3.40	NUM
eurjchem-1000	134	13	%	%	NOUN
eurjchem-1000	134	14	.	.	PUNCT
eurjchem-1000	135	1	the	the	DET
eurjchem-1000	135	2	inter‐day	inter‐day	NOUN
eurjchem-1000	135	3	percentages	percentage	NOUN
eurjchem-1000	135	4	of	of	ADP
eurjchem-1000	135	5	nominal	nominal	ADJ
eurjchem-1000	135	6	concentration	concentration	NOUN
eurjchem-1000	135	7	ranged	range	VERB
eurjchem-1000	135	8	between	between	ADP
eurjchem-1000	135	9	90.90	90.90	NUM
eurjchem-1000	135	10	,	,	PUNCT
eurjchem-1000	135	11	97.30	97.30	NUM
eurjchem-1000	135	12	and	and	CCONJ
eurjchem-1000	135	13	98.90	98.90	NUM
eurjchem-1000	135	14	%	%	NOUN
eurjchem-1000	135	15	.	.	PUNCT
eurjchem-1000	136	1	results	result	NOUN
eurjchem-1000	136	2	are	be	AUX
eurjchem-1000	136	3	presented	present	VERB
eurjchem-1000	136	4	in	in	ADP
eurjchem-1000	136	5	table	table	NOUN
eurjchem-1000	136	6	4	4	NUM
eurjchem-1000	136	7	.	.	PUNCT
eurjchem-1000	137	1	3.2.5	3.2.5	NUM
eurjchem-1000	137	2	.	.	PUNCT
eurjchem-1000	137	3	extraction	extraction	NOUN
eurjchem-1000	137	4	efficiency	efficiency	NOUN
eurjchem-1000	137	5	recovery	recovery	NOUN
eurjchem-1000	137	6	of	of	ADP
eurjchem-1000	137	7	azithromycin	azithromycin	PROPN
eurjchem-1000	137	8	was	be	AUX
eurjchem-1000	137	9	evaluated	evaluate	VERB
eurjchem-1000	137	10	by	by	ADP
eurjchem-1000	137	11	comparing	compare	VERB
eurjchem-1000	137	12	mean	mean	ADJ
eurjchem-1000	137	13	analyte	analyte	NOUN
eurjchem-1000	137	14	responses	response	NOUN
eurjchem-1000	137	15	of	of	ADP
eurjchem-1000	137	16	two	two	NUM
eurjchem-1000	137	17	processed	process	VERB
eurjchem-1000	137	18	samples	sample	NOUN
eurjchem-1000	137	19	of	of	ADP
eurjchem-1000	137	20	low	low	ADJ
eurjchem-1000	137	21	(	(	PUNCT
eurjchem-1000	137	22	qcl	qcl	NOUN
eurjchem-1000	137	23	)	)	PUNCT
eurjchem-1000	137	24	,	,	PUNCT
eurjchem-1000	137	25	medium	medium	NOUN
eurjchem-1000	137	26	(	(	PUNCT
eurjchem-1000	137	27	qcm	qcm	NOUN
eurjchem-1000	137	28	)	)	PUNCT
eurjchem-1000	137	29	and	and	CCONJ
eurjchem-1000	137	30	high	high	ADJ
eurjchem-1000	137	31	(	(	PUNCT
eurjchem-1000	137	32	qch	qch	NOUN
eurjchem-1000	137	33	)	)	PUNCT
eurjchem-1000	137	34	quality	quality	NOUN
eurjchem-1000	137	35	control	control	NOUN
eurjchem-1000	137	36	samples	sample	NOUN
eurjchem-1000	137	37	to	to	PART
eurjchem-1000	137	38	mean	mean	VERB
eurjchem-1000	137	39	analyte	analyte	NOUN
eurjchem-1000	137	40	responses	response	NOUN
eurjchem-1000	137	41	of	of	ADP
eurjchem-1000	137	42	the	the	DET
eurjchem-1000	137	43	same	same	ADJ
eurjchem-1000	137	44	concentrations	concentration	NOUN
eurjchem-1000	137	45	with	with	ADP
eurjchem-1000	137	46	spiked	spiked	ADJ
eurjchem-1000	137	47	samples	sample	NOUN
eurjchem-1000	137	48	in	in	ADP
eurjchem-1000	137	49	previously	previously	ADV
eurjchem-1000	137	50	extracted	extract	VERB
eurjchem-1000	137	51	blank	blank	ADJ
eurjchem-1000	137	52	plasma	plasma	NOUN
eurjchem-1000	137	53	.	.	PUNCT
eurjchem-1000	138	1	mean	mean	VERB
eurjchem-1000	138	2	recovery	recovery	NOUN
eurjchem-1000	138	3	values	value	NOUN
eurjchem-1000	138	4	are	be	AUX
eurjchem-1000	138	5	89.08	89.08	NUM
eurjchem-1000	138	6	,	,	PUNCT
eurjchem-1000	138	7	97.02	97.02	NUM
eurjchem-1000	138	8	and	and	CCONJ
eurjchem-1000	138	9	95.03	95.03	NUM
eurjchem-1000	138	10	%	%	NOUN
eurjchem-1000	138	11	at	at	ADP
eurjchem-1000	138	12	low	low	ADJ
eurjchem-1000	138	13	,	,	PUNCT
eurjchem-1000	138	14	medium	medium	ADJ
eurjchem-1000	138	15	and	and	CCONJ
eurjchem-1000	138	16	high	high	ADJ
eurjchem-1000	138	17	quality	quality	NOUN
eurjchem-1000	138	18	control	control	NOUN
eurjchem-1000	138	19	levels	level	NOUN
eurjchem-1000	138	20	,	,	PUNCT
eurjchem-1000	138	21	respectively	respectively	ADV
eurjchem-1000	138	22	.	.	PUNCT
eurjchem-1000	139	1	results	result	NOUN
eurjchem-1000	139	2	are	be	AUX
eurjchem-1000	139	3	presented	present	VERB
eurjchem-1000	139	4	in	in	ADP
eurjchem-1000	139	5	table	table	NOUN
eurjchem-1000	139	6	5	5	NUM
eurjchem-1000	139	7	.	.	X
eurjchem-1000	139	8	3.2.6	3.2.6	NUM
eurjchem-1000	139	9	.	.	PUNCT
eurjchem-1000	139	10	dilution	dilution	NOUN
eurjchem-1000	139	11	integrity	integrity	NOUN
eurjchem-1000	139	12	three	three	NUM
eurjchem-1000	139	13	replicates	replicate	NOUN
eurjchem-1000	139	14	of	of	ADP
eurjchem-1000	139	15	the	the	DET
eurjchem-1000	139	16	high	high	ADJ
eurjchem-1000	139	17	quality	quality	NOUN
eurjchem-1000	139	18	control	control	NOUN
eurjchem-1000	139	19	(	(	PUNCT
eurjchem-1000	139	20	qch	qch	NOUN
eurjchem-1000	139	21	)	)	PUNCT
eurjchem-1000	139	22	were	be	AUX
eurjchem-1000	139	23	diluted	dilute	VERB
eurjchem-1000	139	24	five	five	NUM
eurjchem-1000	139	25	times	time	NOUN
eurjchem-1000	139	26	in	in	ADP
eurjchem-1000	139	27	human	human	ADJ
eurjchem-1000	139	28	plasma	plasma	NOUN
eurjchem-1000	139	29	prior	prior	ADV
eurjchem-1000	139	30	to	to	ADP
eurjchem-1000	139	31	sample	sample	NOUN
eurjchem-1000	139	32	processing	processing	NOUN
eurjchem-1000	139	33	and	and	CCONJ
eurjchem-1000	139	34	analysis	analysis	NOUN
eurjchem-1000	139	35	.	.	PUNCT
eurjchem-1000	140	1	the	the	DET
eurjchem-1000	140	2	calculated	calculated	ADJ
eurjchem-1000	140	3	concentrations	concentration	NOUN
eurjchem-1000	140	4	,	,	PUNCT
eurjchem-1000	140	5	including	include	VERB
eurjchem-1000	140	6	the	the	DET
eurjchem-1000	140	7	dilution	dilution	NOUN
eurjchem-1000	140	8	factor	factor	NOUN
eurjchem-1000	140	9	,	,	PUNCT
eurjchem-1000	140	10	yielded	yield	VERB
eurjchem-1000	140	11	coefficients	coefficient	NOUN
eurjchem-1000	140	12	of	of	ADP
eurjchem-1000	140	13	variation	variation	NOUN
eurjchem-1000	140	14	of	of	ADP
eurjchem-1000	140	15	4.48	4.48	NUM
eurjchem-1000	140	16	%	%	NOUN
eurjchem-1000	140	17	for	for	ADP
eurjchem-1000	140	18	qch	qch	NOUN
eurjchem-1000	140	19	.	.	PUNCT
eurjchem-1000	141	1	percentages	percentage	NOUN
eurjchem-1000	141	2	of	of	ADP
eurjchem-1000	141	3	nominal	nominal	ADJ
eurjchem-1000	141	4	concentration	concentration	NOUN
eurjchem-1000	141	5	are	be	AUX
eurjchem-1000	141	6	100.67	100.67	NUM
eurjchem-1000	141	7	%	%	NOUN
eurjchem-1000	141	8	results	result	NOUN
eurjchem-1000	141	9	are	be	AUX
eurjchem-1000	141	10	presented	present	VERB
eurjchem-1000	141	11	in	in	ADP
eurjchem-1000	141	12	table	table	NOUN
eurjchem-1000	141	13	6	6	NUM
eurjchem-1000	141	14	.	.	PUNCT
eurjchem-1000	142	1	3.2.7	3.2.7	NUM
eurjchem-1000	142	2	.	.	PUNCT
eurjchem-1000	143	1	stability	stability	NOUN
eurjchem-1000	143	2	studies	study	NOUN
eurjchem-1000	143	3	3.2.7.1	3.2.7.1	NUM
eurjchem-1000	143	4	post‐preparative	post‐preparative	ADJ
eurjchem-1000	143	5	stability	stability	NOUN
eurjchem-1000	143	6	at	at	ADP
eurjchem-1000	143	7	10	10	NUM
eurjchem-1000	143	8	°	°	NOUN
eurjchem-1000	143	9	c	c	NOUN
eurjchem-1000	143	10	samples	sample	NOUN
eurjchem-1000	143	11	prepared	prepare	VERB
eurjchem-1000	143	12	at	at	ADP
eurjchem-1000	143	13	low	low	ADJ
eurjchem-1000	143	14	(	(	PUNCT
eurjchem-1000	143	15	qcl	qcl	NOUN
eurjchem-1000	143	16	)	)	PUNCT
eurjchem-1000	143	17	,	,	PUNCT
eurjchem-1000	143	18	medium	medium	NOUN
eurjchem-1000	143	19	(	(	PUNCT
eurjchem-1000	143	20	qcm	qcm	NOUN
eurjchem-1000	143	21	)	)	PUNCT
eurjchem-1000	143	22	and	and	CCONJ
eurjchem-1000	143	23	high	high	ADJ
eurjchem-1000	143	24	(	(	PUNCT
eurjchem-1000	143	25	qch	qch	NOUN
eurjchem-1000	143	26	)	)	PUNCT
eurjchem-1000	143	27	quality	quality	NOUN
eurjchem-1000	143	28	control	control	NOUN
eurjchem-1000	143	29	levels	level	NOUN
eurjchem-1000	143	30	were	be	AUX
eurjchem-1000	143	31	aliquoted	aliquote	VERB
eurjchem-1000	143	32	and	and	CCONJ
eurjchem-1000	143	33	submitted	submit	VERB
eurjchem-1000	143	34	to	to	ADP
eurjchem-1000	143	35	the	the	DET
eurjchem-1000	143	36	sample	sample	NOUN
eurjchem-1000	143	37	processing	processing	NOUN
eurjchem-1000	143	38	procedure	procedure	NOUN
eurjchem-1000	143	39	and	and	CCONJ
eurjchem-1000	143	40	kept	keep	VERB
eurjchem-1000	143	41	at	at	ADP
eurjchem-1000	143	42	10	10	NUM
eurjchem-1000	143	43	°	°	ADP
eurjchem-1000	143	44	c	c	NOUN
eurjchem-1000	143	45	(	(	PUNCT
eurjchem-1000	143	46	stability	stability	NOUN
eurjchem-1000	143	47	samples	sample	NOUN
eurjchem-1000	143	48	)	)	PUNCT
eurjchem-1000	143	49	.	.	PUNCT
eurjchem-1000	144	1	younes	younes	PROPN
eurjchem-1000	144	2	and	and	CCONJ
eurjchem-1000	144	3	el‐kady	el‐kady	PROPN
eurjchem-1000	144	4	/	/	SYM
eurjchem-1000	144	5	european	european	PROPN
eurjchem-1000	144	6	journal	journal	PROPN
eurjchem-1000	144	7	of	of	ADP
eurjchem-1000	144	8	chemistry	chemistry	NOUN
eurjchem-1000	144	9	5	5	NUM
eurjchem-1000	144	10	(	(	PUNCT
eurjchem-1000	144	11	2	2	NUM
eurjchem-1000	144	12	)	)	PUNCT
eurjchem-1000	144	13	(	(	PUNCT
eurjchem-1000	144	14	2014	2014	NUM
eurjchem-1000	144	15	)	)	PUNCT
eurjchem-1000	144	16	241‐246	241‐246	NUM
eurjchem-1000	144	17	245	245	NUM
eurjchem-1000	144	18	table	table	NOUN
eurjchem-1000	144	19	4	4	NUM
eurjchem-1000	144	20	.	.	PUNCT
eurjchem-1000	144	21	inter‐day	inter‐day	NOUN
eurjchem-1000	144	22	accuracy	accuracy	NOUN
eurjchem-1000	144	23	and	and	CCONJ
eurjchem-1000	144	24	precision	precision	NOUN
eurjchem-1000	144	25	.	.	PUNCT
eurjchem-1000	145	1	day	day	NOUN
eurjchem-1000	145	2	run	run	NOUN
eurjchem-1000	145	3	number	number	NOUN
eurjchem-1000	145	4	qcl	qcl	PROPN
eurjchem-1000	145	5	10	10	NUM
eurjchem-1000	145	6	ng	ng	NOUN
eurjchem-1000	145	7	/	/	SYM
eurjchem-1000	145	8	ml	ml	AUX
eurjchem-1000	145	9	qcm	qcm	VERB
eurjchem-1000	145	10	400	400	NUM
eurjchem-1000	145	11	ng	ng	NOUN
eurjchem-1000	145	12	/	/	SYM
eurjchem-1000	145	13	ml	ml	NOUN
eurjchem-1000	145	14	qch	qch	NOUN
eurjchem-1000	145	15	1200	1200	NUM
eurjchem-1000	145	16	ng	ng	PROPN
eurjchem-1000	145	17	/	/	SYM
eurjchem-1000	145	18	ml	ml	NOUN
eurjchem-1000	145	19	conc	conc	VERB
eurjchem-1000	145	20	.	.	PUNCT
eurjchem-1000	146	1	found	find	VERB
eurjchem-1000	146	2	(	(	PUNCT
eurjchem-1000	146	3	ng	ng	NOUN
eurjchem-1000	146	4	/	/	SYM
eurjchem-1000	146	5	ml	ml	NOUN
eurjchem-1000	146	6	)	)	PUNCT
eurjchem-1000	146	7	%	%	NOUN
eurjchem-1000	146	8	nominal	nominal	ADJ
eurjchem-1000	146	9	conc	conc	NOUN
eurjchem-1000	146	10	.	.	PUNCT
eurjchem-1000	147	1	conc	conc	VERB
eurjchem-1000	147	2	.	.	PUNCT
eurjchem-1000	148	1	found	find	VERB
eurjchem-1000	148	2	(	(	PUNCT
eurjchem-1000	148	3	ng	ng	NOUN
eurjchem-1000	148	4	/	/	SYM
eurjchem-1000	148	5	ml	ml	NOUN
eurjchem-1000	148	6	)	)	PUNCT
eurjchem-1000	148	7	%	%	NOUN
eurjchem-1000	148	8	nominal	nominal	ADJ
eurjchem-1000	148	9	conc	conc	NOUN
eurjchem-1000	148	10	.	.	PUNCT
eurjchem-1000	149	1	conc	conc	VERB
eurjchem-1000	149	2	.	.	PUNCT
eurjchem-1000	150	1	found	find	VERB
eurjchem-1000	150	2	(	(	PUNCT
eurjchem-1000	150	3	ng	ng	NOUN
eurjchem-1000	150	4	/	/	SYM
eurjchem-1000	150	5	ml	ml	NOUN
eurjchem-1000	150	6	)	)	PUNCT
eurjchem-1000	150	7	%	%	NOUN
eurjchem-1000	150	8	nominal	nominal	ADJ
eurjchem-1000	150	9	conc	conc	NOUN
eurjchem-1000	150	10	.	.	PUNCT
eurjchem-1000	151	1	i	i	PRON
eurjchem-1000	151	2	1	1	NUM
eurjchem-1000	151	3	8.3	8.3	NUM
eurjchem-1000	151	4	83.2	83.2	NUM
eurjchem-1000	151	5	385.0	385.0	NUM
eurjchem-1000	151	6	96.3	96.3	NUM
eurjchem-1000	151	7	1203.0	1203.0	NUM
eurjchem-1000	151	8	100.3	100.3	NUM
eurjchem-1000	151	9	2	2	NUM
eurjchem-1000	151	10	8.4	8.4	NUM
eurjchem-1000	151	11	84.0	84.0	NUM
eurjchem-1000	151	12	386.0	386.0	NUM
eurjchem-1000	151	13	96.5	96.5	NUM
eurjchem-1000	151	14	1205.0	1205.0	NUM
eurjchem-1000	151	15	100.4	100.4	NUM
eurjchem-1000	151	16	3	3	NUM
eurjchem-1000	151	17	9.0	9.0	NUM
eurjchem-1000	151	18	90.0	90.0	NUM
eurjchem-1000	151	19	397.0	397.0	NUM
eurjchem-1000	151	20	99.3	99.3	NUM
eurjchem-1000	151	21	1220.0	1220.0	NUM
eurjchem-1000	151	22	101.7	101.7	NUM
eurjchem-1000	151	23	4	4	NUM
eurjchem-1000	151	24	10.0	10.0	NUM
eurjchem-1000	151	25	100.0	100.0	NUM
eurjchem-1000	151	26	375.0	375.0	NUM
eurjchem-1000	151	27	93.8	93.8	NUM
eurjchem-1000	151	28	1159.0	1159.0	NUM
eurjchem-1000	151	29	96.6	96.6	NUM
eurjchem-1000	151	30	5	5	NUM
eurjchem-1000	151	31	10.8	10.8	NUM
eurjchem-1000	151	32	108.0	108.0	NUM
eurjchem-1000	151	33	402.0	402.0	NUM
eurjchem-1000	151	34	100.5	100.5	NUM
eurjchem-1000	151	35	1156.0	1156.0	NUM
eurjchem-1000	151	36	96.3	96.3	NUM
eurjchem-1000	151	37	6	6	NUM
eurjchem-1000	151	38	11.3	11.3	NUM
eurjchem-1000	151	39	113.0	113.0	NUM
eurjchem-1000	151	40	406.0	406.0	NUM
eurjchem-1000	151	41	101.5	101.5	NUM
eurjchem-1000	151	42	1148.0	1148.0	NUM
eurjchem-1000	151	43	95.7	95.7	NUM
eurjchem-1000	151	44	ii	ii	NUM
eurjchem-1000	151	45	1	1	NUM
eurjchem-1000	151	46	10.4	10.4	NUM
eurjchem-1000	151	47	103.6	103.6	NUM
eurjchem-1000	151	48	410.0	410.0	NUM
eurjchem-1000	151	49	102.5	102.5	NUM
eurjchem-1000	151	50	1149.0	1149.0	NUM
eurjchem-1000	151	51	95.8	95.8	NUM
eurjchem-1000	151	52	2	2	NUM
eurjchem-1000	151	53	10.0	10.0	NUM
eurjchem-1000	151	54	100.0	100.0	NUM
eurjchem-1000	151	55	412.0	412.0	NUM
eurjchem-1000	151	56	103.0	103.0	NUM
eurjchem-1000	151	57	1157.0	1157.0	NUM
eurjchem-1000	151	58	96.4	96.4	NUM
eurjchem-1000	151	59	3	3	NUM
eurjchem-1000	151	60	11.2	11.2	NUM
eurjchem-1000	151	61	112.0	112.0	NUM
eurjchem-1000	151	62	416.0	416.0	NUM
eurjchem-1000	151	63	104.0	104.0	NUM
eurjchem-1000	151	64	1169.0	1169.0	NUM
eurjchem-1000	151	65	97.4	97.4	NUM
eurjchem-1000	151	66	4	4	NUM
eurjchem-1000	151	67	9.0	9.0	NUM
eurjchem-1000	151	68	90.0	90.0	NUM
eurjchem-1000	151	69	384.0	384.0	NUM
eurjchem-1000	151	70	96.0	96.0	NUM
eurjchem-1000	151	71	1158.0	1158.0	NUM
eurjchem-1000	151	72	96.5	96.5	NUM
eurjchem-1000	151	73	5	5	NUM
eurjchem-1000	151	74	7.0	7.0	NUM
eurjchem-1000	151	75	70.0	70.0	NUM
eurjchem-1000	151	76	365.0	365.0	NUM
eurjchem-1000	151	77	91.3	91.3	NUM
eurjchem-1000	151	78	1126.0	1126.0	NUM
eurjchem-1000	151	79	93.8	93.8	NUM
eurjchem-1000	151	80	6	6	NUM
eurjchem-1000	151	81	8.0	8.0	NUM
eurjchem-1000	151	82	80.0	80.0	NUM
eurjchem-1000	151	83	372.0	372.0	NUM
eurjchem-1000	151	84	93.0	93.0	NUM
eurjchem-1000	151	85	1136.0	1136.0	NUM
eurjchem-1000	151	86	94.7	94.7	NUM
eurjchem-1000	151	87	iii	iii	NUM
eurjchem-1000	151	88	1	1	NUM
eurjchem-1000	151	89	9.9	9.9	NUM
eurjchem-1000	151	90	98.5	98.5	NUM
eurjchem-1000	151	91	379.0	379.0	NUM
eurjchem-1000	151	92	94.8	94.8	NUM
eurjchem-1000	151	93	1187.0	1187.0	NUM
eurjchem-1000	151	94	98.9	98.9	NUM
eurjchem-1000	151	95	2	2	NUM
eurjchem-1000	151	96	8.5	8.5	NUM
eurjchem-1000	151	97	85.0	85.0	NUM
eurjchem-1000	151	98	377.0	377.0	NUM
eurjchem-1000	151	99	94.3	94.3	NUM
eurjchem-1000	151	100	1214.0	1214.0	NUM
eurjchem-1000	151	101	101.2	101.2	NUM
eurjchem-1000	151	102	3	3	NUM
eurjchem-1000	151	103	7.6	7.6	NUM
eurjchem-1000	151	104	76.0	76.0	NUM
eurjchem-1000	151	105	388.0	388.0	NUM
eurjchem-1000	151	106	97.0	97.0	NUM
eurjchem-1000	151	107	1256.0	1256.0	NUM
eurjchem-1000	151	108	104.7	104.7	NUM
eurjchem-1000	151	109	4	4	NUM
eurjchem-1000	151	110	7.4	7.4	NUM
eurjchem-1000	151	111	74.0	74.0	NUM
eurjchem-1000	151	112	397.0	397.0	NUM
eurjchem-1000	151	113	99.3	99.3	NUM
eurjchem-1000	151	114	1236.0	1236.0	NUM
eurjchem-1000	151	115	103.0	103.0	NUM
eurjchem-1000	151	116	5	5	NUM
eurjchem-1000	151	117	7.9	7.9	NUM
eurjchem-1000	151	118	79.0	79.0	NUM
eurjchem-1000	151	119	346.0	346.0	NUM
eurjchem-1000	151	120	86.5	86.5	NUM
eurjchem-1000	151	121	1245.0	1245.0	NUM
eurjchem-1000	151	122	103.8	103.8	NUM
eurjchem-1000	151	123	6	6	NUM
eurjchem-1000	151	124	8.9	8.9	NUM
eurjchem-1000	151	125	89.0	89.0	NUM
eurjchem-1000	151	126	406.0	406.0	NUM
eurjchem-1000	151	127	101.5	101.5	NUM
eurjchem-1000	151	128	1233.0	1233.0	NUM
eurjchem-1000	151	129	102.8	102.8	NUM
eurjchem-1000	151	130	n	n	NUM
eurjchem-1000	151	131	6.0	6.0	NUM
eurjchem-1000	151	132	6.0	6.0	NUM
eurjchem-1000	151	133	6.0	6.0	NUM
eurjchem-1000	151	134	6.0	6.0	NUM
eurjchem-1000	151	135	6.0	6.0	NUM
eurjchem-1000	151	136	6.0	6.0	NUM
eurjchem-1000	151	137	mean	mean	NOUN
eurjchem-1000	151	138	9.1	9.1	NUM
eurjchem-1000	151	139	90.9	90.9	NUM
eurjchem-1000	151	140	389.1	389.1	NUM
eurjchem-1000	151	141	97.3	97.3	NUM
eurjchem-1000	151	142	1186.5	1186.5	NUM
eurjchem-1000	151	143	98.9	98.9	NUM
eurjchem-1000	151	144	sd	sd	NOUN
eurjchem-1000	151	145	(	(	PUNCT
eurjchem-1000	151	146	±	±	NOUN
eurjchem-1000	151	147	)	)	PUNCT
eurjchem-1000	151	148	1.3	1.3	NUM
eurjchem-1000	151	149	18.4	18.4	NUM
eurjchem-1000	151	150	40.7	40.7	NUM
eurjchem-1000	151	151	cv	cv	NOUN
eurjchem-1000	151	152	(	(	PUNCT
eurjchem-1000	151	153	%	%	NOUN
eurjchem-1000	151	154	)	)	PUNCT
eurjchem-1000	151	155	14.5	14.5	NUM
eurjchem-1000	151	156	4.7	4.7	NUM
eurjchem-1000	151	157	3.4	3.4	NUM
eurjchem-1000	151	158	table	table	NOUN
eurjchem-1000	151	159	5	5	NUM
eurjchem-1000	151	160	.	.	PUNCT
eurjchem-1000	151	161	recovery	recovery	NOUN
eurjchem-1000	151	162	of	of	ADP
eurjchem-1000	151	163	azithromycin	azithromycin	PROPN
eurjchem-1000	151	164	.	.	PUNCT
eurjchem-1000	152	1	extracted	extract	VERB
eurjchem-1000	152	2	sample	sample	NOUN
eurjchem-1000	152	3	analyte	analyte	NOUN
eurjchem-1000	152	4	response	response	NOUN
eurjchem-1000	152	5	theoretical	theoretical	ADJ
eurjchem-1000	152	6	true	true	ADJ
eurjchem-1000	152	7	spiked	spiked	ADJ
eurjchem-1000	152	8	in	in	ADP
eurjchem-1000	152	9	matrix	matrix	NOUN
eurjchem-1000	152	10	analyte	analyte	NOUN
eurjchem-1000	152	11	response	response	NOUN
eurjchem-1000	152	12	analyte	analyte	NOUN
eurjchem-1000	152	13	samples	sample	VERB
eurjchem-1000	152	14	analyte	analyte	NOUN
eurjchem-1000	152	15	3analyte	3analyte	NUM
eurjchem-1000	152	16	2	2	NUM
eurjchem-1000	152	17	analyte	analyte	NOUN
eurjchem-1000	152	18	1analyte	1analyte	NUM
eurjchem-1000	152	19	3analyte	3analyte	NUM
eurjchem-1000	152	20	2analyte	2analyte	NUM
eurjchem-1000	152	21	1	1	NUM
eurjchem-1000	152	22	2854712	2854712	NUM
eurjchem-1000	152	23	945876	945876	NUM
eurjchem-1000	152	24	16598	16598	NUM
eurjchem-1000	152	25	2854126	2854126	NUM
eurjchem-1000	152	26	987541	987541	NUM
eurjchem-1000	152	27	18562	18562	NUM
eurjchem-1000	152	28	sample	sample	NOUN
eurjchem-1000	152	29	1	1	NUM
eurjchem-1000	152	30	2685471	2685471	NUM
eurjchem-1000	152	31	952147	952147	NUM
eurjchem-1000	152	32	14856	14856	NUM
eurjchem-1000	152	33	2963514	2963514	NUM
eurjchem-1000	152	34	965147	965147	NUM
eurjchem-1000	152	35	17451	17451	NUM
eurjchem-1000	152	36	sample	sample	NOUN
eurjchem-1000	152	37	2	2	NUM
eurjchem-1000	152	38	2596874	2596874	NUM
eurjchem-1000	152	39	963214	963214	NUM
eurjchem-1000	152	40	19657	19657	NUM
eurjchem-1000	152	41	2745214	2745214	NUM
eurjchem-1000	152	42	996321	996321	NUM
eurjchem-1000	152	43	21365	21365	NUM
eurjchem-1000	152	44	sample	sample	NOUN
eurjchem-1000	152	45	3	3	NUM
eurjchem-1000	152	46	3	3	NUM
eurjchem-1000	152	47	3	3	NUM
eurjchem-1000	152	48	3	3	NUM
eurjchem-1000	152	49	3	3	NUM
eurjchem-1000	152	50	3	3	NUM
eurjchem-1000	152	51	3	3	NUM
eurjchem-1000	152	52	n	n	PROPN
eurjchem-1000	152	53	2712352.33	2712352.33	NUM
eurjchem-1000	152	54	953745.667	953745.667	NUM
eurjchem-1000	152	55	17037.00	17037.00	NUM
eurjchem-1000	152	56	2854284.667	2854284.667	NUM
eurjchem-1000	152	57	983003	983003	NUM
eurjchem-1000	152	58	19126.00	19126.00	NUM
eurjchem-1000	152	59	mean	mean	VERB
eurjchem-1000	152	60	131004.058	131004.058	NUM
eurjchem-1000	152	61	8778.85883	8778.85883	NOUN
eurjchem-1000	152	62	2430.42	2430.42	NUM
eurjchem-1000	152	63	109150.0865	109150.0865	NUM
eurjchem-1000	152	64	16074.81421	16074.81421	NUM
eurjchem-1000	152	65	2017.03	2017.03	NUM
eurjchem-1000	152	66	sd	sd	ADP
eurjchem-1000	152	67	(	(	PUNCT
eurjchem-1000	152	68	±	±	NOUN
eurjchem-1000	152	69	)	)	PUNCT
eurjchem-1000	152	70	4.83	4.83	NUM
eurjchem-1000	152	71	0.92	0.92	NUM
eurjchem-1000	152	72	14.27	14.27	NUM
eurjchem-1000	152	73	3.82	3.82	NUM
eurjchem-1000	152	74	1.64	1.64	NUM
eurjchem-1000	152	75	10.55	10.55	NUM
eurjchem-1000	152	76	cv	cv	PROPN
eurjchem-1000	152	77	(	(	PUNCT
eurjchem-1000	152	78	%	%	NOUN
eurjchem-1000	152	79	)	)	PUNCT
eurjchem-1000	152	80	1200	1200	NUM
eurjchem-1000	152	81	400	400	NUM
eurjchem-1000	152	82	10	10	NUM
eurjchem-1000	152	83	1200	1200	NUM
eurjchem-1000	152	84	400	400	NUM
eurjchem-1000	152	85	10	10	NUM
eurjchem-1000	152	86	concentration	concentration	NOUN
eurjchem-1000	152	87	(	(	PUNCT
eurjchem-1000	152	88	ng	ng	NOUN
eurjchem-1000	152	89	/	/	SYM
eurjchem-1000	152	90	ml	ml	PROPN
eurjchem-1000	152	91	)	)	PUNCT
eurjchem-1000	153	1	95.03	95.03	NUM
eurjchem-1000	153	2	97.02	97.02	NUM
eurjchem-1000	153	3	89.08	89.08	NUM
eurjchem-1000	153	4	mean	mean	NOUN
eurjchem-1000	153	5	recovery	recovery	NOUN
eurjchem-1000	153	6	(	(	PUNCT
eurjchem-1000	153	7	%	%	INTJ
eurjchem-1000	153	8	)	)	PUNCT
eurjchem-1000	153	9	table	table	NOUN
eurjchem-1000	153	10	6	6	NUM
eurjchem-1000	153	11	.	.	PUNCT
eurjchem-1000	153	12	results	result	NOUN
eurjchem-1000	153	13	of	of	ADP
eurjchem-1000	153	14	dilution	dilution	NOUN
eurjchem-1000	153	15	integrity	integrity	NOUN
eurjchem-1000	153	16	.	.	PUNCT
eurjchem-1000	154	1	analyte	analyte	NOUN
eurjchem-1000	154	2	samples	sample	NOUN
eurjchem-1000	154	3	conc	conc	VERB
eurjchem-1000	154	4	.	.	PUNCT
eurjchem-1000	155	1	vound	vound	PROPN
eurjchem-1000	155	2	(	(	PUNCT
eurjchem-1000	155	3	ng	ng	PROPN
eurjchem-1000	155	4	/	/	SYM
eurjchem-1000	155	5	ml	ml	NOUN
eurjchem-1000	155	6	)	)	PUNCT
eurjchem-1000	155	7	%	%	NOUN
eurjchem-1000	155	8	nominal	nominal	ADJ
eurjchem-1000	155	9	concentration	concentration	NOUN
eurjchem-1000	155	10	sample	sample	NOUN
eurjchem-1000	155	11	1	1	NUM
eurjchem-1000	155	12	1156.00	1156.00	NUM
eurjchem-1000	155	13	96.33	96.33	NUM
eurjchem-1000	155	14	sample	sample	NOUN
eurjchem-1000	155	15	2	2	NUM
eurjchem-1000	155	16	1204.00	1204.00	NUM
eurjchem-1000	155	17	100.33	100.33	NUM
eurjchem-1000	155	18	sample	sample	NOUN
eurjchem-1000	155	19	3	3	NUM
eurjchem-1000	155	20	1264.00	1264.00	NUM
eurjchem-1000	155	21	105.33	105.33	NUM
eurjchem-1000	155	22	n	n	PRON
eurjchem-1000	155	23	3	3	NUM
eurjchem-1000	155	24	3	3	NUM
eurjchem-1000	155	25	mean	mean	NOUN
eurjchem-1000	155	26	1208.00	1208.00	NUM
eurjchem-1000	155	27	100.67	100.67	NUM
eurjchem-1000	155	28	sd	sd	NOUN
eurjchem-1000	155	29	(	(	PUNCT
eurjchem-1000	155	30	±	±	PROPN
eurjchem-1000	155	31	)	)	PUNCT
eurjchem-1000	155	32	54.11	54.11	NUM
eurjchem-1000	155	33	cv	cv	PROPN
eurjchem-1000	155	34	(	(	PUNCT
eurjchem-1000	155	35	%	%	NOUN
eurjchem-1000	155	36	)	)	PUNCT
eurjchem-1000	155	37	4.48	4.48	NUM
eurjchem-1000	155	38	three	three	NUM
eurjchem-1000	155	39	replicates	replicate	NOUN
eurjchem-1000	155	40	of	of	ADP
eurjchem-1000	155	41	those	those	DET
eurjchem-1000	155	42	quality	quality	NOUN
eurjchem-1000	155	43	control	control	NOUN
eurjchem-1000	155	44	samples	sample	NOUN
eurjchem-1000	155	45	were	be	AUX
eurjchem-1000	155	46	freshly	freshly	ADV
eurjchem-1000	155	47	processed	process	VERB
eurjchem-1000	155	48	with	with	ADP
eurjchem-1000	155	49	a	a	DET
eurjchem-1000	155	50	calibration	calibration	NOUN
eurjchem-1000	155	51	curve	curve	NOUN
eurjchem-1000	155	52	and	and	CCONJ
eurjchem-1000	155	53	analyzed	analyze	VERB
eurjchem-1000	155	54	in	in	ADP
eurjchem-1000	155	55	a	a	DET
eurjchem-1000	155	56	single	single	ADJ
eurjchem-1000	155	57	run	run	NOUN
eurjchem-1000	155	58	to	to	PART
eurjchem-1000	155	59	serve	serve	VERB
eurjchem-1000	155	60	as	as	ADP
eurjchem-1000	155	61	time	time	NOUN
eurjchem-1000	155	62	zero	zero	NUM
eurjchem-1000	155	63	(	(	PUNCT
eurjchem-1000	155	64	comparison	comparison	NOUN
eurjchem-1000	155	65	samples	sample	NOUN
eurjchem-1000	155	66	)	)	PUNCT
eurjchem-1000	155	67	.	.	PUNCT
eurjchem-1000	156	1	after	after	ADP
eurjchem-1000	156	2	100	100	NUM
eurjchem-1000	156	3	hours	hour	NOUN
eurjchem-1000	156	4	,	,	PUNCT
eurjchem-1000	156	5	a	a	DET
eurjchem-1000	156	6	calibration	calibration	NOUN
eurjchem-1000	156	7	curve	curve	NOUN
eurjchem-1000	156	8	was	be	AUX
eurjchem-1000	156	9	freshly	freshly	ADV
eurjchem-1000	156	10	processed	process	VERB
eurjchem-1000	156	11	and	and	CCONJ
eurjchem-1000	156	12	analyzed	analyze	VERB
eurjchem-1000	156	13	with	with	ADP
eurjchem-1000	156	14	all	all	DET
eurjchem-1000	156	15	stability	stability	NOUN
eurjchem-1000	156	16	samples	sample	NOUN
eurjchem-1000	156	17	in	in	ADP
eurjchem-1000	156	18	a	a	DET
eurjchem-1000	156	19	single	single	ADJ
eurjchem-1000	156	20	run	run	NOUN
eurjchem-1000	156	21	.	.	PUNCT
eurjchem-1000	157	1	concentrations	concentration	NOUN
eurjchem-1000	157	2	were	be	AUX
eurjchem-1000	157	3	calculated	calculate	VERB
eurjchem-1000	157	4	to	to	PART
eurjchem-1000	157	5	determine	determine	VERB
eurjchem-1000	157	6	%	%	NOUN
eurjchem-1000	157	7	change	change	NOUN
eurjchem-1000	157	8	after	after	ADP
eurjchem-1000	157	9	100	100	NUM
eurjchem-1000	157	10	hours	hour	NOUN
eurjchem-1000	157	11	when	when	SCONJ
eurjchem-1000	157	12	compared	compare	VERB
eurjchem-1000	157	13	to	to	ADP
eurjchem-1000	157	14	time	time	NOUN
eurjchem-1000	157	15	zero	zero	NUM
eurjchem-1000	157	16	.	.	PUNCT
eurjchem-1000	158	1	azithromycin	azithromycin	PROPN
eurjchem-1000	158	2	is	be	AUX
eurjchem-1000	158	3	found	find	VERB
eurjchem-1000	158	4	to	to	PART
eurjchem-1000	158	5	be	be	AUX
eurjchem-1000	158	6	stable	stable	ADJ
eurjchem-1000	158	7	for	for	ADP
eurjchem-1000	158	8	100	100	NUM
eurjchem-1000	158	9	hours	hour	NOUN
eurjchem-1000	158	10	at	at	ADP
eurjchem-1000	158	11	10	10	NUM
eurjchem-1000	158	12	°	°	ADP
eurjchem-1000	158	13	c	c	NOUN
eurjchem-1000	158	14	following	follow	VERB
eurjchem-1000	158	15	sample	sample	NOUN
eurjchem-1000	158	16	processing	processing	NOUN
eurjchem-1000	158	17	with	with	ADP
eurjchem-1000	158	18	%	%	NOUN
eurjchem-1000	158	19	changes	change	NOUN
eurjchem-1000	158	20	of	of	ADP
eurjchem-1000	158	21	‐9.71	‐9.71	NOUN
eurjchem-1000	158	22	,	,	PUNCT
eurjchem-1000	158	23	‐7.40	‐7.40	NOUN
eurjchem-1000	158	24	and	and	CCONJ
eurjchem-1000	158	25	‐2.68	‐2.68	ADJ
eurjchem-1000	158	26	%	%	NOUN
eurjchem-1000	158	27	.	.	PUNCT
eurjchem-1000	159	1	results	result	NOUN
eurjchem-1000	159	2	are	be	AUX
eurjchem-1000	159	3	presented	present	VERB
eurjchem-1000	159	4	in	in	ADP
eurjchem-1000	159	5	table	table	NOUN
eurjchem-1000	159	6	7	7	NUM
eurjchem-1000	159	7	.	.	PUNCT
eurjchem-1000	159	8	3.2.7.2	3.2.7.2	NUM
eurjchem-1000	159	9	.	.	PUNCT
eurjchem-1000	160	1	short‐term	short‐term	ADJ
eurjchem-1000	160	2	stability	stability	NOUN
eurjchem-1000	160	3	of	of	ADP
eurjchem-1000	160	4	azithromycin	azithromycin	NOUN
eurjchem-1000	160	5	in	in	ADP
eurjchem-1000	160	6	matrix	matrix	NOUN
eurjchem-1000	160	7	at	at	ADP
eurjchem-1000	160	8	room	room	NOUN
eurjchem-1000	160	9	temperature	temperature	NOUN
eurjchem-1000	160	10	samples	sample	NOUN
eurjchem-1000	160	11	were	be	AUX
eurjchem-1000	160	12	prepared	prepare	VERB
eurjchem-1000	160	13	at	at	ADP
eurjchem-1000	160	14	low	low	ADJ
eurjchem-1000	160	15	(	(	PUNCT
eurjchem-1000	160	16	qcl	qcl	NOUN
eurjchem-1000	160	17	)	)	PUNCT
eurjchem-1000	160	18	,	,	PUNCT
eurjchem-1000	160	19	medium	medium	NOUN
eurjchem-1000	160	20	(	(	PUNCT
eurjchem-1000	160	21	qcm	qcm	NOUN
eurjchem-1000	160	22	)	)	PUNCT
eurjchem-1000	160	23	and	and	CCONJ
eurjchem-1000	160	24	high	high	ADJ
eurjchem-1000	160	25	(	(	PUNCT
eurjchem-1000	160	26	qch	qch	NOUN
eurjchem-1000	160	27	)	)	PUNCT
eurjchem-1000	160	28	quality	quality	NOUN
eurjchem-1000	160	29	control	control	NOUN
eurjchem-1000	160	30	levels	level	NOUN
eurjchem-1000	160	31	.	.	PUNCT
eurjchem-1000	161	1	three	three	NUM
eurjchem-1000	161	2	replicates	replicate	NOUN
eurjchem-1000	161	3	of	of	ADP
eurjchem-1000	161	4	low	low	ADJ
eurjchem-1000	161	5	,	,	PUNCT
eurjchem-1000	161	6	medium	medium	ADJ
eurjchem-1000	161	7	and	and	CCONJ
eurjchem-1000	161	8	high	high	ADJ
eurjchem-1000	161	9	quality	quality	NOUN
eurjchem-1000	161	10	control	control	NOUN
eurjchem-1000	161	11	samples	sample	NOUN
eurjchem-1000	161	12	were	be	AUX
eurjchem-1000	161	13	left	leave	VERB
eurjchem-1000	161	14	at	at	ADP
eurjchem-1000	161	15	room	room	NOUN
eurjchem-1000	161	16	(	(	PUNCT
eurjchem-1000	161	17	stability	stability	NOUN
eurjchem-1000	161	18	samples	sample	NOUN
eurjchem-1000	161	19	)	)	PUNCT
eurjchem-1000	161	20	.	.	PUNCT
eurjchem-1000	162	1	three	three	NUM
eurjchem-1000	162	2	replicates	replicate	NOUN
eurjchem-1000	162	3	of	of	ADP
eurjchem-1000	162	4	those	those	DET
eurjchem-1000	162	5	quality	quality	NOUN
eurjchem-1000	162	6	controls	control	NOUN
eurjchem-1000	162	7	samples	sample	NOUN
eurjchem-1000	162	8	were	be	AUX
eurjchem-1000	162	9	freshly	freshly	ADV
eurjchem-1000	162	10	processed	process	VERB
eurjchem-1000	162	11	with	with	ADP
eurjchem-1000	162	12	a	a	DET
eurjchem-1000	162	13	calibration	calibration	NOUN
eurjchem-1000	162	14	curve	curve	NOUN
eurjchem-1000	162	15	and	and	CCONJ
eurjchem-1000	162	16	,	,	PUNCT
eurjchem-1000	162	17	analyzed	analyze	VERB
eurjchem-1000	162	18	in	in	ADP
eurjchem-1000	162	19	a	a	DET
eurjchem-1000	162	20	single	single	ADJ
eurjchem-1000	162	21	run	run	NOUN
eurjchem-1000	162	22	to	to	PART
eurjchem-1000	162	23	serve	serve	VERB
eurjchem-1000	162	24	as	as	ADP
eurjchem-1000	162	25	time	time	NOUN
eurjchem-1000	162	26	zero	zero	NUM
eurjchem-1000	162	27	(	(	PUNCT
eurjchem-1000	162	28	comparison	comparison	NOUN
eurjchem-1000	162	29	samples	sample	NOUN
eurjchem-1000	162	30	)	)	PUNCT
eurjchem-1000	162	31	.	.	PUNCT
eurjchem-1000	163	1	after	after	ADP
eurjchem-1000	163	2	24	24	NUM
eurjchem-1000	163	3	hours	hour	NOUN
eurjchem-1000	163	4	,	,	PUNCT
eurjchem-1000	163	5	a	a	DET
eurjchem-1000	163	6	calibration	calibration	NOUN
eurjchem-1000	163	7	curve	curve	NOUN
eurjchem-1000	163	8	was	be	AUX
eurjchem-1000	163	9	freshly	freshly	ADV
eurjchem-1000	163	10	processed	process	VERB
eurjchem-1000	163	11	and	and	CCONJ
eurjchem-1000	163	12	analyzed	analyze	VERB
eurjchem-1000	163	13	with	with	ADP
eurjchem-1000	163	14	all	all	DET
eurjchem-1000	163	15	stability	stability	NOUN
eurjchem-1000	163	16	samples	sample	NOUN
eurjchem-1000	163	17	in	in	ADP
eurjchem-1000	163	18	a	a	DET
eurjchem-1000	163	19	single	single	ADJ
eurjchem-1000	163	20	run	run	NOUN
eurjchem-1000	163	21	.	.	PUNCT
eurjchem-1000	164	1	concentrations	concentration	NOUN
eurjchem-1000	164	2	were	be	AUX
eurjchem-1000	164	3	calculated	calculate	VERB
eurjchem-1000	164	4	to	to	PART
eurjchem-1000	164	5	determine	determine	VERB
eurjchem-1000	164	6	%	%	NOUN
eurjchem-1000	164	7	change	change	NOUN
eurjchem-1000	164	8	over	over	ADP
eurjchem-1000	164	9	the	the	DET
eurjchem-1000	164	10	time	time	NOUN
eurjchem-1000	164	11	when	when	SCONJ
eurjchem-1000	164	12	compared	compare	VERB
eurjchem-1000	164	13	to	to	ADP
eurjchem-1000	164	14	time	time	NOUN
eurjchem-1000	164	15	zero	zero	NUM
eurjchem-1000	164	16	.	.	PUNCT
eurjchem-1000	165	1	azithromycin	azithromycin	PROPN
eurjchem-1000	165	2	is	be	AUX
eurjchem-1000	165	3	found	find	VERB
eurjchem-1000	165	4	to	to	PART
eurjchem-1000	165	5	be	be	AUX
eurjchem-1000	165	6	stable	stable	ADJ
eurjchem-1000	165	7	in	in	ADP
eurjchem-1000	165	8	human	human	ADJ
eurjchem-1000	165	9	plasma	plasma	NOUN
eurjchem-1000	165	10	for	for	ADP
eurjchem-1000	165	11	24	24	NUM
eurjchem-1000	165	12	hours	hour	NOUN
eurjchem-1000	165	13	at	at	ADP
eurjchem-1000	165	14	room	room	NOUN
eurjchem-1000	165	15	temperature	temperature	NOUN
eurjchem-1000	165	16	with	with	ADP
eurjchem-1000	165	17	%	%	NOUN
eurjchem-1000	165	18	changes	change	NOUN
eurjchem-1000	165	19	of	of	ADP
eurjchem-1000	165	20	‐9.34	‐9.34	NOUN
eurjchem-1000	165	21	,	,	PUNCT
eurjchem-1000	165	22	‐9.03	‐9.03	ADP
eurjchem-1000	165	23	and	and	CCONJ
eurjchem-1000	165	24	‐1.77	‐1.77	NUM
eurjchem-1000	165	25	%	%	NOUN
eurjchem-1000	165	26	.	.	PUNCT
eurjchem-1000	166	1	results	result	NOUN
eurjchem-1000	166	2	are	be	AUX
eurjchem-1000	166	3	presented	present	VERB
eurjchem-1000	166	4	in	in	ADP
eurjchem-1000	166	5	table	table	NOUN
eurjchem-1000	166	6	7	7	NUM
eurjchem-1000	166	7	.	.	PUNCT
eurjchem-1000	166	8	3.2.7.3	3.2.7.3	NUM
eurjchem-1000	166	9	.	.	PUNCT
eurjchem-1000	167	1	freeze	freeze	NOUN
eurjchem-1000	167	2	and	and	CCONJ
eurjchem-1000	167	3	thaw	thaw	NOUN
eurjchem-1000	167	4	stability	stability	NOUN
eurjchem-1000	167	5	at	at	ADP
eurjchem-1000	167	6	‐20	‐20	PROPN
eurjchem-1000	167	7	°	°	PROPN
eurjchem-1000	167	8	c	c	NOUN
eurjchem-1000	167	9	samples	sample	NOUN
eurjchem-1000	167	10	were	be	AUX
eurjchem-1000	167	11	prepared	prepare	VERB
eurjchem-1000	167	12	at	at	ADP
eurjchem-1000	167	13	low	low	ADJ
eurjchem-1000	167	14	(	(	PUNCT
eurjchem-1000	167	15	qcl	qcl	NOUN
eurjchem-1000	167	16	)	)	PUNCT
eurjchem-1000	167	17	,	,	PUNCT
eurjchem-1000	167	18	medium	medium	NOUN
eurjchem-1000	167	19	(	(	PUNCT
eurjchem-1000	167	20	qcm	qcm	NOUN
eurjchem-1000	167	21	)	)	PUNCT
eurjchem-1000	167	22	and	and	CCONJ
eurjchem-1000	167	23	high	high	ADJ
eurjchem-1000	167	24	(	(	PUNCT
eurjchem-1000	167	25	qch	qch	NOUN
eurjchem-1000	167	26	)	)	PUNCT
eurjchem-1000	167	27	quality	quality	NOUN
eurjchem-1000	167	28	control	control	NOUN
eurjchem-1000	167	29	levels	level	NOUN
eurjchem-1000	167	30	,	,	PUNCT
eurjchem-1000	167	31	aliquoted	aliquote	VERB
eurjchem-1000	167	32	and	and	CCONJ
eurjchem-1000	167	33	frozen	freeze	VERB
eurjchem-1000	167	34	at	at	ADP
eurjchem-1000	167	35	‐20	‐20	PROPN
eurjchem-1000	167	36	°	°	ADP
eurjchem-1000	167	37	c	c	NOUN
eurjchem-1000	167	38	.	.	PUNCT
eurjchem-1000	168	1	some	some	PRON
eurjchem-1000	168	2	of	of	ADP
eurjchem-1000	168	3	the	the	DET
eurjchem-1000	168	4	aliquots	aliquot	NOUN
eurjchem-1000	168	5	of	of	ADP
eurjchem-1000	168	6	quality	quality	NOUN
eurjchem-1000	168	7	control	control	NOUN
eurjchem-1000	168	8	samples	sample	NOUN
eurjchem-1000	168	9	were	be	AUX
eurjchem-1000	168	10	subjected	subject	VERB
eurjchem-1000	168	11	to	to	ADP
eurjchem-1000	168	12	three	three	NUM
eurjchem-1000	168	13	freeze‐thaw	freeze‐thaw	NOUN
eurjchem-1000	168	14	cycles	cycle	NOUN
eurjchem-1000	168	15	(	(	PUNCT
eurjchem-1000	168	16	stability	stability	NOUN
eurjchem-1000	168	17	samples	sample	NOUN
eurjchem-1000	168	18	)	)	PUNCT
eurjchem-1000	168	19	.	.	PUNCT
eurjchem-1000	169	1	a	a	DET
eurjchem-1000	169	2	calibration	calibration	NOUN
eurjchem-1000	169	3	curve	curve	NOUN
eurjchem-1000	169	4	and	and	CCONJ
eurjchem-1000	169	5	quality	quality	NOUN
eurjchem-1000	169	6	control	control	NOUN
eurjchem-1000	169	7	samples	sample	NOUN
eurjchem-1000	169	8	were	be	AUX
eurjchem-1000	169	9	freshly	freshly	ADV
eurjchem-1000	169	10	prepared	prepare	VERB
eurjchem-1000	169	11	and	and	CCONJ
eurjchem-1000	169	12	processed	process	VERB
eurjchem-1000	169	13	with	with	ADP
eurjchem-1000	169	14	3	3	NUM
eurjchem-1000	169	15	replicates	replicate	NOUN
eurjchem-1000	169	16	of	of	ADP
eurjchem-1000	169	17	stability	stability	NOUN
eurjchem-1000	169	18	samples	sample	NOUN
eurjchem-1000	169	19	and	and	CCONJ
eurjchem-1000	169	20	analysed	analyse	VERB
eurjchem-1000	169	21	in	in	ADP
eurjchem-1000	169	22	a	a	DET
eurjchem-1000	169	23	single	single	ADJ
eurjchem-1000	169	24	run	run	NOUN
eurjchem-1000	169	25	.	.	PUNCT
eurjchem-1000	170	1	azithromycin	azithromycin	PROPN
eurjchem-1000	170	2	is	be	AUX
eurjchem-1000	170	3	found	find	VERB
eurjchem-1000	170	4	to	to	PART
eurjchem-1000	170	5	be	be	AUX
eurjchem-1000	170	6	stable	stable	ADJ
eurjchem-1000	170	7	in	in	ADP
eurjchem-1000	170	8	human	human	ADJ
eurjchem-1000	170	9	plasma	plasma	NOUN
eurjchem-1000	170	10	after	after	ADP
eurjchem-1000	170	11	three	three	NUM
eurjchem-1000	170	12	freeze‐thaw	freeze‐thaw	NOUN
eurjchem-1000	170	13	cycles	cycle	NOUN
eurjchem-1000	170	14	at	at	ADP
eurjchem-1000	170	15	,	,	PUNCT
eurjchem-1000	170	16	‐20	‐20	PROPN
eurjchem-1000	170	17	°	°	ADP
eurjchem-1000	170	18	c	c	NOUN
eurjchem-1000	170	19	with	with	ADP
eurjchem-1000	170	20	coefficients	coefficient	NOUN
eurjchem-1000	170	21	of	of	ADP
eurjchem-1000	170	22	variation	variation	NOUN
eurjchem-1000	170	23	of	of	ADP
eurjchem-1000	170	24	7.78	7.78	NUM
eurjchem-1000	170	25	,	,	PUNCT
eurjchem-1000	170	26	1.71	1.71	NUM
eurjchem-1000	170	27	and	and	CCONJ
eurjchem-1000	170	28	1.48	1.48	NUM
eurjchem-1000	170	29	%	%	NOUN
eurjchem-1000	170	30	and	and	CCONJ
eurjchem-1000	170	31	nominal	nominal	ADJ
eurjchem-1000	170	32	concentrations	concentration	NOUN
eurjchem-1000	170	33	of	of	ADP
eurjchem-1000	170	34	103.66	103.66	NUM
eurjchem-1000	170	35	,	,	PUNCT
eurjchem-1000	170	36	95.75	95.75	NUM
eurjchem-1000	170	37	and	and	CCONJ
eurjchem-1000	170	38	95.61	95.61	NUM
eurjchem-1000	170	39	%	%	NOUN
eurjchem-1000	170	40	for	for	ADP
eurjchem-1000	170	41	qcl	qcl	NOUN
eurjchem-1000	170	42	,	,	PUNCT
eurjchem-1000	170	43	qcm	qcm	NOUN
eurjchem-1000	170	44	and	and	CCONJ
eurjchem-1000	170	45	qch	qch	NOUN
eurjchem-1000	170	46	,	,	PUNCT
eurjchem-1000	170	47	respectively	respectively	ADV
eurjchem-1000	170	48	.	.	PUNCT
eurjchem-1000	171	1	results	result	NOUN
eurjchem-1000	171	2	are	be	AUX
eurjchem-1000	171	3	presented	present	VERB
eurjchem-1000	171	4	in	in	ADP
eurjchem-1000	171	5	table	table	NOUN
eurjchem-1000	171	6	7	7	NUM
eurjchem-1000	171	7	.	.	PUNCT
eurjchem-1000	172	1	3.2.7.4	3.2.7.4	NUM
eurjchem-1000	172	2	.	.	PUNCT
eurjchem-1000	173	1	long‐term	long‐term	NOUN
eurjchem-1000	173	2	stability	stability	NOUN
eurjchem-1000	173	3	of	of	ADP
eurjchem-1000	173	4	azithromycin	azithromycin	NOUN
eurjchem-1000	173	5	in	in	ADP
eurjchem-1000	173	6	matrix	matrix	NOUN
eurjchem-1000	173	7	at	at	ADP
eurjchem-1000	173	8	‐20	‐20	PROPN
eurjchem-1000	173	9	°	°	PROPN
eurjchem-1000	173	10	c	c	NOUN
eurjchem-1000	173	11	stability	stability	NOUN
eurjchem-1000	173	12	samples	sample	NOUN
eurjchem-1000	173	13	were	be	AUX
eurjchem-1000	173	14	prepared	prepare	VERB
eurjchem-1000	173	15	in	in	ADP
eurjchem-1000	173	16	human	human	ADJ
eurjchem-1000	173	17	plasma	plasma	NOUN
eurjchem-1000	173	18	at	at	ADP
eurjchem-1000	173	19	low	low	ADJ
eurjchem-1000	173	20	(	(	PUNCT
eurjchem-1000	173	21	qcl	qcl	NOUN
eurjchem-1000	173	22	)	)	PUNCT
eurjchem-1000	173	23	,	,	PUNCT
eurjchem-1000	173	24	medium	medium	NOUN
eurjchem-1000	173	25	(	(	PUNCT
eurjchem-1000	173	26	qcm	qcm	NOUN
eurjchem-1000	173	27	)	)	PUNCT
eurjchem-1000	173	28	and	and	CCONJ
eurjchem-1000	173	29	high	high	ADJ
eurjchem-1000	173	30	(	(	PUNCT
eurjchem-1000	173	31	qch	qch	NOUN
eurjchem-1000	173	32	)	)	PUNCT
eurjchem-1000	173	33	quality	quality	NOUN
eurjchem-1000	173	34	control	control	NOUN
eurjchem-1000	173	35	levels	level	NOUN
eurjchem-1000	173	36	and	and	CCONJ
eurjchem-1000	173	37	stored	store	VERB
eurjchem-1000	173	38	at	at	ADP
eurjchem-1000	173	39	‐20	‐20	PROPN
eurjchem-1000	173	40	°	°	ADP
eurjchem-1000	173	41	c	c	X
eurjchem-1000	173	42	(	(	PUNCT
eurjchem-1000	173	43	stability	stability	NOUN
eurjchem-1000	173	44	samples	sample	NOUN
eurjchem-1000	173	45	)	)	PUNCT
eurjchem-1000	173	46	.	.	PUNCT
eurjchem-1000	174	1	246	246	NUM
eurjchem-1000	174	2	younes	youne	NOUN
eurjchem-1000	174	3	and	and	CCONJ
eurjchem-1000	174	4	el‐kady	el‐kady	PROPN
eurjchem-1000	174	5	/	/	SYM
eurjchem-1000	174	6	european	european	PROPN
eurjchem-1000	174	7	journal	journal	PROPN
eurjchem-1000	174	8	of	of	ADP
eurjchem-1000	174	9	chemistry	chemistry	NOUN
eurjchem-1000	174	10	5	5	NUM
eurjchem-1000	174	11	(	(	PUNCT
eurjchem-1000	174	12	2	2	NUM
eurjchem-1000	174	13	)	)	PUNCT
eurjchem-1000	174	14	(	(	PUNCT
eurjchem-1000	174	15	2014	2014	NUM
eurjchem-1000	174	16	)	)	PUNCT
eurjchem-1000	174	17	241‐246	241‐246	NUM
eurjchem-1000	174	18	table	table	NOUN
eurjchem-1000	174	19	7	7	NUM
eurjchem-1000	174	20	.	.	PUNCT
eurjchem-1000	174	21	summary	summary	NOUN
eurjchem-1000	174	22	of	of	ADP
eurjchem-1000	174	23	validation	validation	NOUN
eurjchem-1000	174	24	results	result	NOUN
eurjchem-1000	174	25	.	.	PUNCT
eurjchem-1000	175	1	parameters	parameter	NOUN
eurjchem-1000	175	2	value	value	VERB
eurjchem-1000	175	3	linearity	linearity	NOUN
eurjchem-1000	175	4	r	r	PROPN
eurjchem-1000	175	5	≥	≥	NUM
eurjchem-1000	175	6	0.999	0.999	NUM
eurjchem-1000	175	7	calibration	calibration	NOUN
eurjchem-1000	175	8	curve	curve	NOUN
eurjchem-1000	175	9	range	range	NOUN
eurjchem-1000	175	10	5‐1500	5‐1500	NUM
eurjchem-1000	175	11	ng	ng	PROPN
eurjchem-1000	175	12	/	/	SYM
eurjchem-1000	175	13	ml	ml	NOUN
eurjchem-1000	175	14	inter‐day	inter‐day	PROPN
eurjchem-1000	175	15	accuracy	accuracy	PROPN
eurjchem-1000	175	16	qc	qc	PROPN
eurjchem-1000	175	17	%	%	NOUN
eurjchem-1000	175	18	nominal	nominal	ADJ
eurjchem-1000	175	19	conc	conc	NOUN
eurjchem-1000	175	20	.	.	PUNCT
eurjchem-1000	175	21	,	,	PUNCT
eurjchem-1000	175	22	90.90	90.90	NUM
eurjchem-1000	175	23	,	,	PUNCT
eurjchem-1000	175	24	97.30	97.30	NUM
eurjchem-1000	175	25	and	and	CCONJ
eurjchem-1000	175	26	98.90	98.90	NUM
eurjchem-1000	175	27	%	%	NOUN
eurjchem-1000	175	28	inter‐day	inter‐day	NOUN
eurjchem-1000	175	29	precision	precision	PROPN
eurjchem-1000	175	30	qc	qc	PROPN
eurjchem-1000	175	31	coefficients	coefficient	NOUN
eurjchem-1000	175	32	of	of	ADP
eurjchem-1000	175	33	variation	variation	NOUN
eurjchem-1000	175	34	,	,	PUNCT
eurjchem-1000	175	35	14.50	14.50	NUM
eurjchem-1000	175	36	,	,	PUNCT
eurjchem-1000	175	37	4.70	4.70	NUM
eurjchem-1000	175	38	and	and	CCONJ
eurjchem-1000	175	39	3.40	3.40	NUM
eurjchem-1000	175	40	%	%	NOUN
eurjchem-1000	175	41	intra‐day	intra‐day	NOUN
eurjchem-1000	175	42	accuracy	accuracy	PROPN
eurjchem-1000	175	43	qc	qc	PROPN
eurjchem-1000	175	44	%	%	NOUN
eurjchem-1000	175	45	nominal	nominal	ADJ
eurjchem-1000	175	46	conc	conc	NOUN
eurjchem-1000	175	47	.	.	PUNCT
eurjchem-1000	175	48	,	,	PUNCT
eurjchem-1000	175	49	97.81	97.81	NUM
eurjchem-1000	175	50	,	,	PUNCT
eurjchem-1000	175	51	98.58	98.58	NUM
eurjchem-1000	175	52	and	and	CCONJ
eurjchem-1000	175	53	96.65	96.65	NUM
eurjchem-1000	175	54	%	%	NOUN
eurjchem-1000	175	55	intra‐day	intra‐day	PROPN
eurjchem-1000	175	56	precision	precision	PROPN
eurjchem-1000	175	57	qc	qc	PROPN
eurjchem-1000	175	58	coefficients	coefficient	NOUN
eurjchem-1000	175	59	of	of	ADP
eurjchem-1000	175	60	variation	variation	NOUN
eurjchem-1000	175	61	,	,	PUNCT
eurjchem-1000	175	62	9.29	9.29	NUM
eurjchem-1000	175	63	,	,	PUNCT
eurjchem-1000	175	64	4.28	4.28	NUM
eurjchem-1000	175	65	and	and	CCONJ
eurjchem-1000	175	66	3.16	3.16	NUM
eurjchem-1000	175	67	%	%	NOUN
eurjchem-1000	175	68	recovery	recovery	NOUN
eurjchem-1000	175	69	of	of	ADP
eurjchem-1000	175	70	analyte	analyte	NOUN
eurjchem-1000	175	71	qc	qc	PROPN
eurjchem-1000	175	72	means	means	PROPN
eurjchem-1000	175	73	,	,	PUNCT
eurjchem-1000	175	74	89.08	89.08	NUM
eurjchem-1000	175	75	,	,	PUNCT
eurjchem-1000	175	76	97.02	97.02	NUM
eurjchem-1000	175	77	and	and	CCONJ
eurjchem-1000	175	78	95.03	95.03	NUM
eurjchem-1000	175	79	%	%	NOUN
eurjchem-1000	175	80	lower	low	ADJ
eurjchem-1000	175	81	limit	limit	NOUN
eurjchem-1000	175	82	of	of	ADP
eurjchem-1000	175	83	quantification	quantification	NOUN
eurjchem-1000	175	84	5	5	NUM
eurjchem-1000	175	85	ng	ng	PROPN
eurjchem-1000	175	86	/	/	SYM
eurjchem-1000	175	87	ml	ml	NOUN
eurjchem-1000	175	88	dilution	dilution	NOUN
eurjchem-1000	175	89	integrity	integrity	NOUN
eurjchem-1000	175	90	accuracy	accuracy	NOUN
eurjchem-1000	175	91	qc	qc	PROPN
eurjchem-1000	175	92	%	%	PROPN
eurjchem-1000	175	93	nominal	nominal	NOUN
eurjchem-1000	175	94	.	.	PUNCT
eurjchem-1000	176	1	cone	cone	PROPN
eurjchem-1000	176	2	.	.	PUNCT
eurjchem-1000	176	3	,	,	PUNCT
eurjchem-1000	176	4	100.67	100.67	NUM
eurjchem-1000	176	5	%	%	NOUN
eurjchem-1000	176	6	dilution	dilution	NOUN
eurjchem-1000	176	7	integrity	integrity	NOUN
eurjchem-1000	176	8	precision	precision	PROPN
eurjchem-1000	176	9	qc	qc	PROPN
eurjchem-1000	176	10	coefficient	coefficient	NOUN
eurjchem-1000	176	11	of	of	ADP
eurjchem-1000	176	12	variation	variation	NOUN
eurjchem-1000	176	13	,	,	PUNCT
eurjchem-1000	176	14	4.48	4.48	NUM
eurjchem-1000	176	15	%	%	NOUN
eurjchem-1000	176	16	post‐preparative	post‐preparative	ADJ
eurjchem-1000	176	17	stability	stability	NOUN
eurjchem-1000	176	18	at	at	ADP
eurjchem-1000	176	19	10	10	NUM
eurjchem-1000	176	20	°	°	NOUN
eurjchem-1000	176	21	c	c	NOUN
eurjchem-1000	176	22	mean	mean	NOUN
eurjchem-1000	176	23	%	%	NOUN
eurjchem-1000	176	24	change	change	NOUN
eurjchem-1000	176	25	,	,	PUNCT
eurjchem-1000	176	26	‐9.71	‐9.71	NOUN
eurjchem-1000	176	27	,	,	PUNCT
eurjchem-1000	176	28	‐7.40	‐7.40	NOUN
eurjchem-1000	176	29	and	and	CCONJ
eurjchem-1000	176	30	‐2.68	‐2.68	ADJ
eurjchem-1000	176	31	%	%	NOUN
eurjchem-1000	176	32	short‐term	short‐term	ADJ
eurjchem-1000	176	33	stability	stability	NOUN
eurjchem-1000	176	34	of	of	ADP
eurjchem-1000	176	35	analyte	analyte	NOUN
eurjchem-1000	176	36	in	in	ADP
eurjchem-1000	176	37	matrix	matrix	NOUN
eurjchem-1000	176	38	at	at	ADP
eurjchem-1000	176	39	‐20	‐20	PROPN
eurjchem-1000	176	40	°	°	PROPN
eurjchem-1000	176	41	c	c	NOUN
eurjchem-1000	176	42	mean	mean	NOUN
eurjchem-1000	176	43	%	%	NOUN
eurjchem-1000	176	44	change	change	NOUN
eurjchem-1000	176	45	after	after	ADP
eurjchem-1000	176	46	24	24	NUM
eurjchem-1000	176	47	hours	hour	NOUN
eurjchem-1000	176	48	,	,	PUNCT
eurjchem-1000	176	49	‐9.34	‐9.34	NOUN
eurjchem-1000	176	50	,	,	PUNCT
eurjchem-1000	176	51	‐9.03	‐9.03	ADP
eurjchem-1000	176	52	and	and	CCONJ
eurjchem-1000	176	53	‐1.77	‐1.77	NUM
eurjchem-1000	176	54	%	%	NOUN
eurjchem-1000	176	55	long‐term	long‐term	NOUN
eurjchem-1000	176	56	stability	stability	NOUN
eurjchem-1000	176	57	of	of	ADP
eurjchem-1000	176	58	analyte	analyte	NOUN
eurjchem-1000	176	59	in	in	ADP
eurjchem-1000	176	60	matrix	matrix	NOUN
eurjchem-1000	176	61	at	at	ADP
eurjchem-1000	176	62	‐20	‐20	PROPN
eurjchem-1000	176	63	°	°	PROPN
eurjchem-1000	176	64	c	c	NOUN
eurjchem-1000	176	65	mean	mean	NOUN
eurjchem-1000	176	66	%	%	NOUN
eurjchem-1000	176	67	change	change	NOUN
eurjchem-1000	176	68	after	after	ADP
eurjchem-1000	176	69	52	52	NUM
eurjchem-1000	176	70	days	day	NOUN
eurjchem-1000	176	71	,	,	PUNCT
eurjchem-1000	176	72	‐11.12	‐11.12	NOUN
eurjchem-1000	176	73	,	,	PUNCT
eurjchem-1000	176	74	‐7.09	‐7.09	NUM
eurjchem-1000	176	75	and	and	CCONJ
eurjchem-1000	176	76	‐3.05	‐3.05	NUM
eurjchem-1000	176	77	%	%	NOUN
eurjchem-1000	176	78	freeze	freeze	NOUN
eurjchem-1000	176	79	and	and	CCONJ
eurjchem-1000	176	80	thaw	thaw	NOUN
eurjchem-1000	176	81	stability	stability	NOUN
eurjchem-1000	176	82	of	of	ADP
eurjchem-1000	176	83	analyte	analyte	NOUN
eurjchem-1000	176	84	in	in	ADP
eurjchem-1000	176	85	matrix	matrix	NOUN
eurjchem-1000	176	86	at	at	ADP
eurjchem-1000	176	87	‐20	‐20	PROPN
eurjchem-1000	176	88	°	°	PROPN
eurjchem-1000	176	89	c	c	PROPN
eurjchem-1000	176	90	qc	qc	PROPN
eurjchem-1000	176	91	%	%	NOUN
eurjchem-1000	176	92	nominal	nominal	ADJ
eurjchem-1000	176	93	conc	conc	NOUN
eurjchem-1000	176	94	.	.	PUNCT
eurjchem-1000	176	95	,	,	PUNCT
eurjchem-1000	176	96	103.66	103.66	NUM
eurjchem-1000	176	97	,	,	PUNCT
eurjchem-1000	176	98	95.75	95.75	NUM
eurjchem-1000	176	99	and	and	CCONJ
eurjchem-1000	176	100	95.61	95.61	NUM
eurjchem-1000	176	101	%	%	NOUN
eurjchem-1000	176	102	a	a	DET
eurjchem-1000	176	103	calibration	calibration	NOUN
eurjchem-1000	176	104	curve	curve	NOUN
eurjchem-1000	176	105	and	and	CCONJ
eurjchem-1000	176	106	3	3	NUM
eurjchem-1000	176	107	replicates	replicate	NOUN
eurjchem-1000	176	108	of	of	ADP
eurjchem-1000	176	109	low	low	ADJ
eurjchem-1000	176	110	and	and	CCONJ
eurjchem-1000	176	111	high	high	ADJ
eurjchem-1000	176	112	quality	quality	NOUN
eurjchem-1000	176	113	control	control	NOUN
eurjchem-1000	176	114	samples	sample	NOUN
eurjchem-1000	176	115	(	(	PUNCT
eurjchem-1000	176	116	comparison	comparison	NOUN
eurjchem-1000	176	117	samples	sample	NOUN
eurjchem-1000	176	118	)	)	PUNCT
eurjchem-1000	176	119	were	be	AUX
eurjchem-1000	176	120	freshly	freshly	ADV
eurjchem-1000	176	121	processed	process	VERB
eurjchem-1000	176	122	with	with	ADP
eurjchem-1000	176	123	three	three	NUM
eurjchem-1000	176	124	replicates	replicate	NOUN
eurjchem-1000	176	125	of	of	ADP
eurjchem-1000	176	126	stability	stability	NOUN
eurjchem-1000	176	127	samples	sample	NOUN
eurjchem-1000	176	128	and	and	CCONJ
eurjchem-1000	176	129	analysed	analyse	VERB
eurjchem-1000	176	130	in	in	ADP
eurjchem-1000	176	131	a	a	DET
eurjchem-1000	176	132	single	single	ADJ
eurjchem-1000	176	133	run	run	NOUN
eurjchem-1000	176	134	.	.	PUNCT
eurjchem-1000	177	1	concentrations	concentration	NOUN
eurjchem-1000	177	2	were	be	AUX
eurjchem-1000	177	3	calculated	calculate	VERB
eurjchem-1000	177	4	to	to	PART
eurjchem-1000	177	5	determine	determine	VERB
eurjchem-1000	177	6	%	%	NOUN
eurjchem-1000	177	7	change	change	NOUN
eurjchem-1000	177	8	over	over	ADP
eurjchem-1000	177	9	time	time	NOUN
eurjchem-1000	177	10	.	.	PUNCT
eurjchem-1000	178	1	azithromycin	azithromycin	PROPN
eurjchem-1000	178	2	is	be	AUX
eurjchem-1000	178	3	found	find	VERB
eurjchem-1000	178	4	to	to	PART
eurjchem-1000	178	5	be	be	AUX
eurjchem-1000	178	6	stable	stable	ADJ
eurjchem-1000	178	7	in	in	ADP
eurjchem-1000	178	8	human	human	ADJ
eurjchem-1000	178	9	plasma	plasma	NOUN
eurjchem-1000	178	10	for	for	ADP
eurjchem-1000	178	11	52	52	NUM
eurjchem-1000	178	12	days	day	NOUN
eurjchem-1000	178	13	at	at	ADP
eurjchem-1000	178	14	‐20	‐20	PROPN
eurjchem-1000	178	15	°	°	ADP
eurjchem-1000	178	16	c	c	NOUN
eurjchem-1000	178	17	with	with	ADP
eurjchem-1000	178	18	%	%	NOUN
eurjchem-1000	178	19	changes	change	NOUN
eurjchem-1000	178	20	of	of	ADP
eurjchem-1000	178	21	‐11.12	‐11.12	NOUN
eurjchem-1000	178	22	,	,	PUNCT
eurjchem-1000	178	23	‐7.09	‐7.09	NUM
eurjchem-1000	178	24	and	and	CCONJ
eurjchem-1000	178	25	‐3.05	‐3.05	NUM
eurjchem-1000	178	26	%	%	NOUN
eurjchem-1000	178	27	.	.	PUNCT
eurjchem-1000	179	1	results	result	NOUN
eurjchem-1000	179	2	are	be	AUX
eurjchem-1000	179	3	presented	present	VERB
eurjchem-1000	179	4	in	in	ADP
eurjchem-1000	179	5	table	table	NOUN
eurjchem-1000	179	6	7	7	NUM
eurjchem-1000	179	7	.	.	NOUN
eurjchem-1000	179	8	4	4	NUM
eurjchem-1000	179	9	.	.	X
eurjchem-1000	179	10	conclusion	conclusion	NOUN
eurjchem-1000	179	11	the	the	DET
eurjchem-1000	179	12	developed	develop	VERB
eurjchem-1000	179	13	lc‐ms	lc‐ms	AUX
eurjchem-1000	179	14	/	/	SYM
eurjchem-1000	179	15	ms	ms	PROPN
eurjchem-1000	179	16	assay	assay	PROPN
eurjchem-1000	179	17	for	for	ADP
eurjchem-1000	179	18	azithromycin	azithromycin	PROPN
eurjchem-1000	179	19	is	be	AUX
eurjchem-1000	179	20	rapid	rapid	ADJ
eurjchem-1000	179	21	,	,	PUNCT
eurjchem-1000	179	22	selective	selective	ADJ
eurjchem-1000	179	23	,	,	PUNCT
eurjchem-1000	179	24	and	and	CCONJ
eurjchem-1000	179	25	suitable	suitable	ADJ
eurjchem-1000	179	26	for	for	ADP
eurjchem-1000	179	27	routine	routine	ADJ
eurjchem-1000	179	28	measurement	measurement	NOUN
eurjchem-1000	179	29	of	of	ADP
eurjchem-1000	179	30	subject	subject	ADJ
eurjchem-1000	179	31	samples	sample	NOUN
eurjchem-1000	179	32	.	.	PUNCT
eurjchem-1000	180	1	this	this	DET
eurjchem-1000	180	2	study	study	NOUN
eurjchem-1000	180	3	reports	report	VERB
eurjchem-1000	180	4	a	a	DET
eurjchem-1000	180	5	high	high	ADJ
eurjchem-1000	180	6	throughput	throughput	NOUN
eurjchem-1000	180	7	liquid‐liquid	liquid‐liquid	NOUN
eurjchem-1000	180	8	extraction	extraction	NOUN
eurjchem-1000	180	9	method	method	NOUN
eurjchem-1000	180	10	for	for	ADP
eurjchem-1000	180	11	extraction	extraction	NOUN
eurjchem-1000	180	12	of	of	ADP
eurjchem-1000	180	13	azithromycin	azithromycin	NOUN
eurjchem-1000	180	14	in	in	ADP
eurjchem-1000	180	15	human	human	ADJ
eurjchem-1000	180	16	plasma	plasma	NOUN
eurjchem-1000	180	17	using	use	VERB
eurjchem-1000	180	18	lc‐ms	lc‐ms	AUX
eurjchem-1000	180	19	/	/	SYM
eurjchem-1000	180	20	ms	ms	PROPN
eurjchem-1000	180	21	.	.	PROPN
eurjchem-1000	181	1	the	the	DET
eurjchem-1000	181	2	developed	develop	VERB
eurjchem-1000	181	3	method	method	NOUN
eurjchem-1000	181	4	provided	provide	VERB
eurjchem-1000	181	5	a	a	DET
eurjchem-1000	181	6	short	short	ADJ
eurjchem-1000	181	7	run	run	NOUN
eurjchem-1000	181	8	time	time	NOUN
eurjchem-1000	181	9	of	of	ADP
eurjchem-1000	181	10	about	about	ADV
eurjchem-1000	181	11	0.5	0.5	NUM
eurjchem-1000	181	12	minutes	minute	NOUN
eurjchem-1000	181	13	that	that	PRON
eurjchem-1000	181	14	can	can	AUX
eurjchem-1000	181	15	afford	afford	VERB
eurjchem-1000	181	16	the	the	DET
eurjchem-1000	181	17	analysis	analysis	NOUN
eurjchem-1000	181	18	of	of	ADP
eurjchem-1000	181	19	more	more	ADJ
eurjchem-1000	181	20	than	than	ADP
eurjchem-1000	181	21	400	400	NUM
eurjchem-1000	181	22	plasma	plasma	NOUN
eurjchem-1000	181	23	samples	sample	NOUN
eurjchem-1000	181	24	per	per	ADP
eurjchem-1000	181	25	day	day	NOUN
eurjchem-1000	181	26	.	.	PUNCT
eurjchem-1000	182	1	the	the	DET
eurjchem-1000	182	2	present	present	ADJ
eurjchem-1000	182	3	method	method	NOUN
eurjchem-1000	182	4	also	also	ADV
eurjchem-1000	182	5	provided	provide	VERB
eurjchem-1000	182	6	excellent	excellent	ADJ
eurjchem-1000	182	7	specificity	specificity	NOUN
eurjchem-1000	182	8	and	and	CCONJ
eurjchem-1000	182	9	linearity	linearity	NOUN
eurjchem-1000	182	10	with	with	ADP
eurjchem-1000	182	11	an	an	DET
eurjchem-1000	182	12	lloq	lloq	NOUN
eurjchem-1000	182	13	of	of	ADP
eurjchem-1000	182	14	5	5	NUM
eurjchem-1000	182	15	ng	ng	NOUN
eurjchem-1000	182	16	/	/	SYM
eurjchem-1000	182	17	ml	ml	NOUN
eurjchem-1000	182	18	for	for	ADP
eurjchem-1000	182	19	azithromycin	azithromycin	NOUN
eurjchem-1000	182	20	.	.	PUNCT
eurjchem-1000	183	1	acknowledgement	acknowledgement	NOUN
eurjchem-1000	183	2	the	the	DET
eurjchem-1000	183	3	authors	author	NOUN
eurjchem-1000	183	4	thank	thank	VERB
eurjchem-1000	183	5	the	the	DET
eurjchem-1000	183	6	holding	hold	VERB
eurjchem-1000	183	7	company	company	NOUN
eurjchem-1000	183	8	for	for	ADP
eurjchem-1000	183	9	biological	biological	ADJ
eurjchem-1000	183	10	products	product	NOUN
eurjchem-1000	183	11	and	and	CCONJ
eurjchem-1000	183	12	vaccines	vaccine	NOUN
eurjchem-1000	183	13	(	(	PUNCT
eurjchem-1000	183	14	vacsera	vacsera	PROPN
eurjchem-1000	183	15	)	)	PUNCT
eurjchem-1000	183	16	,	,	PUNCT
eurjchem-1000	183	17	cairo	cairo	PROPN
eurjchem-1000	183	18	,	,	PUNCT
eurjchem-1000	183	19	egypt	egypt	PROPN
eurjchem-1000	183	20	,	,	PUNCT
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eurjchem-1000	183	25	.	.	PUNCT
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eurjchem-1000	184	3	1	1	NUM
eurjchem-1000	184	4	]	]	PUNCT
eurjchem-1000	184	5	.	.	PUNCT
eurjchem-1000	185	1	reynolds	reynolds	PROPN
eurjchem-1000	185	2	,	,	PUNCT
eurjchem-1000	185	3	j.	j.	PROPN
eurjchem-1000	185	4	e.	e.	PROPN
eurjchem-1000	185	5	f.	f.	PROPN
eurjchem-1000	185	6	(	(	PUNCT
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eurjchem-1000	185	8	.	.	PUNCT
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eurjchem-1000	185	10	,	,	PUNCT
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eurjchem-1000	185	12	:	:	PUNCT
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eurjchem-1000	185	14	extra	extra	ADJ
eurjchem-1000	185	15	pharmacopoeia	pharmacopoeia	NOUN
eurjchem-1000	185	16	,	,	PUNCT
eurjchem-1000	185	17	36th	36th	ADJ
eurjchem-1000	185	18	edition	edition	NOUN
eurjchem-1000	185	19	,	,	PUNCT
eurjchem-1000	185	20	the	the	DET
eurjchem-1000	185	21	pharmaceutical	pharmaceutical	NOUN
eurjchem-1000	185	22	press	press	NOUN
eurjchem-1000	185	23	,	,	PUNCT
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eurjchem-1000	185	25	,	,	PUNCT
eurjchem-1000	185	26	2009	2009	NUM
eurjchem-1000	185	27	,	,	PUNCT
eurjchem-1000	185	28	207	207	NUM
eurjchem-1000	185	29	.	.	PUNCT
eurjchem-1000	186	1	[	[	X
eurjchem-1000	186	2	2	2	NUM
eurjchem-1000	186	3	]	]	PUNCT
eurjchem-1000	186	4	.	.	PUNCT
eurjchem-1000	186	5	ghodsi	ghodsi	PROPN
eurjchem-1000	186	6	,	,	PUNCT
eurjchem-1000	186	7	r.	r.	PROPN
eurjchem-1000	186	8	;	;	PUNCT
eurjchem-1000	186	9	kobarfard	kobarfard	PROPN
eurjchem-1000	186	10	,	,	PUNCT
eurjchem-1000	186	11	k.	k.	PROPN
eurjchem-1000	186	12	;	;	PUNCT
eurjchem-1000	186	13	tabatabai	tabatabai	PROPN
eurjchem-1000	186	14	s.	s.	PROPN
eurjchem-1000	186	15	a.	a.	PROPN
eurjchem-1000	186	16	iranian	iranian	PROPN
eurjchem-1000	186	17	j.	j.	PROPN
eurjchem-1000	186	18	pharm	pharm	PROPN
eurjchem-1000	186	19	.	.	PUNCT
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eurjchem-1000	187	2	.	.	PROPN
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eurjchem-1000	187	4	,	,	PUNCT
eurjchem-1000	187	5	11	11	NUM
eurjchem-1000	187	6	,	,	PUNCT
eurjchem-1000	187	7	123‐127	123‐127	NUM
eurjchem-1000	187	8	.	.	PUNCT
eurjchem-1000	188	1	[	[	X
eurjchem-1000	188	2	3	3	NUM
eurjchem-1000	188	3	]	]	PUNCT
eurjchem-1000	188	4	.	.	PUNCT
eurjchem-1000	188	5	suhagia	suhagia	PROPN
eurjchem-1000	188	6	,	,	PUNCT
eurjchem-1000	188	7	b.	b.	PROPN
eurjchem-1000	188	8	n.	n.	PROPN
eurjchem-1000	188	9	;	;	PUNCT
eurjchem-1000	188	10	shah	shah	PROPN
eurjchem-1000	188	11	,	,	PUNCT
eurjchem-1000	188	12	s.	s.	PROPN
eurjchem-1000	188	13	a.	a.	PROPN
eurjchem-1000	188	14	;	;	PUNCT
eurjchem-1000	188	15	rathod	rathod	PROPN
eurjchem-1000	188	16	,	,	PUNCT
eurjchem-1000	188	17	i.	i.	PROPN
eurjchem-1000	188	18	s.	s.	PROPN
eurjchem-1000	188	19	;	;	PUNCT
eurjchem-1000	188	20	patel	patel	PROPN
eurjchem-1000	188	21	,	,	PUNCT
eurjchem-1000	188	22	h.	h.	PROPN
eurjchem-1000	188	23	m.	m.	PROPN
eurjchem-1000	188	24	;	;	PUNCT
eurjchem-1000	188	25	doshi	doshi	PROPN
eurjchem-1000	188	26	,	,	PUNCT
eurjchem-1000	188	27	k.	k.	PROPN
eurjchem-1000	188	28	r.	r.	PROPN
eurjchem-1000	188	29	indian	indian	PROPN
eurjchem-1000	188	30	j.	j.	PROPN
eurjchem-1000	188	31	pharm	pharm	PROPN
eurjchem-1000	188	32	.	.	PUNCT
eurjchem-1000	189	1	sci	sci	PROPN
eurjchem-1000	189	2	.	.	PROPN
eurjchem-1000	189	3	2006	2006	NUM
eurjchem-1000	189	4	,	,	PUNCT
eurjchem-1000	189	5	68	68	NUM
eurjchem-1000	189	6	,	,	PUNCT
eurjchem-1000	189	7	242‐245	242‐245	NUM
eurjchem-1000	189	8	.	.	PUNCT
eurjchem-1000	190	1	[	[	X
eurjchem-1000	190	2	4	4	NUM
eurjchem-1000	190	3	]	]	PUNCT
eurjchem-1000	190	4	.	.	PUNCT
eurjchem-1000	191	1	mallah	mallah	PROPN
eurjchem-1000	191	2	,	,	PUNCT
eurjchem-1000	191	3	m.	m.	NOUN
eurjchem-1000	191	4	a.	a.	PROPN
eurjchem-1000	191	5	;	;	PUNCT
eurjchem-1000	191	6	sherazi	sherazi	PROPN
eurjchem-1000	191	7	,	,	PUNCT
eurjchem-1000	191	8	s.	s.	PROPN
eurjchem-1000	191	9	t.	t.	PROPN
eurjchem-1000	191	10	h.	h.	PROPN
eurjchem-1000	191	11	;	;	PUNCT
eurjchem-1000	191	12	mahesar	mahesar	PROPN
eurjchem-1000	191	13	,	,	PUNCT
eurjchem-1000	191	14	s.	s.	PROPN
eurjchem-1000	191	15	a.	a.	PROPN
eurjchem-1000	191	16	;	;	PUNCT
eurjchem-1000	191	17	rauf	rauf	PROPN
eurjchem-1000	191	18	,	,	PUNCT
eurjchem-1000	191	19	a.	a.	PROPN
eurjchem-1000	191	20	pak	pak	PROPN
eurjchem-1000	191	21	.	.	PUNCT
eurjchem-1000	192	1	j.	j.	PROPN
eurjchem-1000	192	2	anal	anal	PROPN
eurjchem-1000	192	3	.	.	PUNCT
eurjchem-1000	193	1	environ	environ	PROPN
eurjchem-1000	193	2	.	.	PUNCT
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eurjchem-1000	193	4	.	.	PUNCT
eurjchem-1000	194	1	2011	2011	NUM
eurjchem-1000	194	2	,	,	PUNCT
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eurjchem-1000	194	4	,	,	PUNCT
eurjchem-1000	194	5	61‐67	61‐67	ADJ
eurjchem-1000	194	6	.	.	PUNCT
eurjchem-1000	195	1	[	[	X
eurjchem-1000	195	2	5	5	NUM
eurjchem-1000	195	3	]	]	PUNCT
eurjchem-1000	195	4	.	.	PUNCT
eurjchem-1000	196	1	khashaba	khashaba	PROPN
eurjchem-1000	196	2	,	,	PUNCT
eurjchem-1000	196	3	p.	p.	PROPN
eurjchem-1000	196	4	y.	y.	PROPN
eurjchem-1000	196	5	j.	j.	PROPN
eurjchem-1000	196	6	pharm	pharm	PROPN
eurjchem-1000	196	7	.	.	PUNCT
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eurjchem-1000	196	9	.	.	PUNCT
eurjchem-1000	197	1	anal	anal	PROPN
eurjchem-1000	197	2	.	.	PUNCT
eurjchem-1000	198	1	2002	2002	NUM
eurjchem-1000	198	2	,	,	PUNCT
eurjchem-1000	198	3	27	27	NUM
eurjchem-1000	198	4	,	,	PUNCT
eurjchem-1000	198	5	923‐932	923‐932	NUM
eurjchem-1000	198	6	.	.	PUNCT
eurjchem-1000	199	1	[	[	X
eurjchem-1000	199	2	6	6	NUM
eurjchem-1000	199	3	]	]	PUNCT
eurjchem-1000	199	4	.	.	PUNCT
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eurjchem-1000	199	6	,	,	PUNCT
eurjchem-1000	199	7	t.	t.	PROPN
eurjchem-1000	199	8	j.	j.	PROPN
eurjchem-1000	199	9	;	;	PUNCT
eurjchem-1000	199	10	guchelaar	guchelaar	NOUN
eurjchem-1000	199	11	,	,	PUNCT
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eurjchem-1000	199	13	j.	j.	PROPN
eurjchem-1000	199	14	j.	j.	PROPN
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eurjchem-1000	199	16	b.	b.	PROPN
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eurjchem-1000	199	18	,	,	PUNCT
eurjchem-1000	199	19	720	720	NUM
eurjchem-1000	199	20	,	,	PUNCT
eurjchem-1000	199	21	89‐97	89‐97	NUM
eurjchem-1000	199	22	.	.	PUNCT
eurjchem-1000	200	1	[	[	X
eurjchem-1000	200	2	7	7	NUM
eurjchem-1000	200	3	]	]	SYM
eurjchem-1000	200	4	.	.	PUNCT
eurjchem-1000	200	5	bahrami	bahrami	PROPN
eurjchem-1000	200	6	,	,	PUNCT
eurjchem-1000	200	7	g.	g.	PROPN
eurjchem-1000	200	8	;	;	PUNCT
eurjchem-1000	200	9	mirzae	mirzae	PROPN
eurjchem-1000	200	10	,	,	PUNCT
eurjchem-1000	200	11	s.	s.	PROPN
eurjchem-1000	200	12	;	;	PUNCT
eurjchem-1000	200	13	kiani	kiani	PROPN
eurjchem-1000	200	14	,	,	PUNCT
eurjchem-1000	200	15	a.	a.	PROPN
eurjchem-1000	200	16	j.	j.	PROPN
eurjchem-1000	200	17	chromatogr	chromatogr	PROPN
eurjchem-1000	200	18	b.	b.	PROPN
eurjchem-1000	200	19	2005	2005	NUM
eurjchem-1000	200	20	,	,	PUNCT
eurjchem-1000	200	21	820	820	NUM
eurjchem-1000	200	22	,	,	PUNCT
eurjchem-1000	200	23	277‐281	277‐281	NUM
eurjchem-1000	200	24	.	.	PUNCT
eurjchem-1000	201	1	[	[	X
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eurjchem-1000	201	4	.	.	PUNCT
eurjchem-1000	201	5	bahrami	bahrami	PROPN
eurjchem-1000	201	6	,	,	PUNCT
eurjchem-1000	201	7	g.	g.	PROPN
eurjchem-1000	201	8	;	;	PUNCT
eurjchem-1000	201	9	mohammadi	mohammadi	NOUN
eurjchem-1000	201	10	,	,	PUNCT
eurjchem-1000	201	11	b.	b.	PROPN
eurjchem-1000	201	12	j.	j.	PROPN
eurjchem-1000	201	13	chromatogr	chromatogr	PROPN
eurjchem-1000	201	14	b.	b.	PROPN
eurjchem-1000	201	15	2006	2006	NUM
eurjchem-1000	201	16	,	,	PUNCT
eurjchem-1000	201	17	830	830	NUM
eurjchem-1000	201	18	,	,	PUNCT
eurjchem-1000	201	19	355‐358	355‐358	PROPN
eurjchem-1000	201	20	.	.	PUNCT
eurjchem-1000	202	1	[	[	X
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eurjchem-1000	202	3	]	]	PUNCT
eurjchem-1000	202	4	.	.	PUNCT
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eurjchem-1000	203	2	,	,	PUNCT
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eurjchem-1000	203	4	;	;	PUNCT
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eurjchem-1000	203	6	,	,	PUNCT
eurjchem-1000	203	7	h.	h.	PROPN
eurjchem-1000	203	8	;	;	PUNCT
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eurjchem-1000	203	10	,	,	PUNCT
eurjchem-1000	203	11	e.	e.	PROPN
eurjchem-1000	203	12	;	;	PUNCT
eurjchem-1000	203	13	kotaki	kotaki	PROPN
eurjchem-1000	203	14	,	,	PUNCT
eurjchem-1000	203	15	h.	h.	PROPN
eurjchem-1000	203	16	;	;	PUNCT
eurjchem-1000	203	17	sato	sato	PROPN
eurjchem-1000	203	18	,	,	PUNCT
eurjchem-1000	203	19	h.	h.	PROPN
eurjchem-1000	203	20	;	;	PUNCT
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eurjchem-1000	203	26	b.	b.	PROPN
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eurjchem-1000	203	28	,	,	PUNCT
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eurjchem-1000	203	30	,	,	PUNCT
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eurjchem-1000	204	3	]	]	PUNCT
eurjchem-1000	204	4	.	.	PUNCT
eurjchem-1000	205	1	palomeque	palomeque	PROPN
eurjchem-1000	205	2	,	,	PUNCT
eurjchem-1000	205	3	m.	m.	PROPN
eurjchem-1000	205	4	e.	e.	PROPN
eurjchem-1000	205	5	;	;	PUNCT
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eurjchem-1000	205	7	,	,	PUNCT
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eurjchem-1000	205	12	,	,	PUNCT
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eurjchem-1000	205	14	,	,	PUNCT
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eurjchem-1000	205	16	.	.	PUNCT
eurjchem-1000	206	1	[	[	X
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eurjchem-1000	206	3	]	]	PUNCT
eurjchem-1000	206	4	.	.	PUNCT
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eurjchem-1000	207	2	,	,	PUNCT
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eurjchem-1000	207	4	;	;	PUNCT
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eurjchem-1000	207	6	,	,	PUNCT
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eurjchem-1000	207	8	;	;	PUNCT
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eurjchem-1000	207	10	,	,	PUNCT
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eurjchem-1000	207	12	j.	j.	PROPN
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eurjchem-1000	207	14	a.	a.	PROPN
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eurjchem-1000	207	16	,	,	PUNCT
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eurjchem-1000	207	18	,	,	PUNCT
eurjchem-1000	207	19	287‐	287‐	NUM
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eurjchem-1000	207	21	.	.	PUNCT
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eurjchem-1000	208	2	12	12	NUM
eurjchem-1000	208	3	]	]	PUNCT
eurjchem-1000	208	4	.	.	PUNCT
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eurjchem-1000	209	5	;	;	PUNCT
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eurjchem-1000	209	10	;	;	PUNCT
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eurjchem-1000	209	13	r.	r.	PROPN
eurjchem-1000	209	14	a.	a.	PROPN
eurjchem-1000	209	15	;	;	PUNCT
eurjchem-1000	209	16	mullins	mullins	PROPN
eurjchem-1000	209	17	,	,	PUNCT
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eurjchem-1000	209	22	.	.	PUNCT
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eurjchem-1000	210	2	,	,	PUNCT
eurjchem-1000	210	3	565	565	NUM
eurjchem-1000	210	4	(	(	PUNCT
eurjchem-1000	210	5	1‐2	1‐2	NUM
eurjchem-1000	210	6	)	)	PUNCT
eurjchem-1000	210	7	,	,	PUNCT
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eurjchem-1000	210	9	.	.	PUNCT
eurjchem-1000	211	1	[	[	X
eurjchem-1000	211	2	13	13	NUM
eurjchem-1000	211	3	]	]	PUNCT
eurjchem-1000	211	4	.	.	PUNCT
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eurjchem-1000	212	2	,	,	PUNCT
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eurjchem-1000	212	4	;	;	PUNCT
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eurjchem-1000	212	6	,	,	PUNCT
eurjchem-1000	212	7	c.	c.	PROPN
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eurjchem-1000	212	9	;	;	PUNCT
eurjchem-1000	212	10	panchagnula	panchagnula	PROPN
eurjchem-1000	212	11	,	,	PUNCT
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eurjchem-1000	212	13	j.	j.	PROPN
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eurjchem-1000	212	15	.	.	PROPN
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eurjchem-1000	212	17	.	.	PUNCT
eurjchem-1000	213	1	anal	anal	ADJ
eurjchem-1000	213	2	.	.	PUNCT
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eurjchem-1000	214	2	,	,	PUNCT
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eurjchem-1000	214	4	,	,	PUNCT
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eurjchem-1000	214	6	.	.	PUNCT
eurjchem-1000	215	1	[	[	X
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eurjchem-1000	215	3	]	]	PUNCT
eurjchem-1000	215	4	.	.	PUNCT
eurjchem-1000	216	1	fouda	fouda	PROPN
eurjchem-1000	216	2	,	,	PUNCT
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eurjchem-1000	216	5	;	;	PUNCT
eurjchem-1000	216	6	schneider	schneider	PROPN
eurjchem-1000	216	7	,	,	PUNCT
eurjchem-1000	216	8	r.	r.	PROPN
eurjchem-1000	216	9	p.	p.	PROPN
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eurjchem-1000	216	11	.	.	PUNCT
eurjchem-1000	217	1	drug	drug	PROPN
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eurjchem-1000	217	3	.	.	PUNCT
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eurjchem-1000	218	2	,	,	PUNCT
eurjchem-1000	218	3	17	17	NUM
eurjchem-1000	218	4	,	,	PUNCT
eurjchem-1000	218	5	179‐183	179‐183	NUM
eurjchem-1000	218	6	.	.	PUNCT
eurjchem-1000	219	1	[	[	X
eurjchem-1000	219	2	15	15	NUM
eurjchem-1000	219	3	]	]	PUNCT
eurjchem-1000	219	4	.	.	PUNCT
eurjchem-1000	219	5	abuin	abuin	PROPN
eurjchem-1000	219	6	,	,	PUNCT
eurjchem-1000	219	7	s.	s.	PROPN
eurjchem-1000	219	8	o.	o.	PROPN
eurjchem-1000	219	9	;	;	PUNCT
eurjchem-1000	219	10	codony	codony	PROPN
eurjchem-1000	219	11	,	,	PUNCT
eurjchem-1000	219	12	r.	r.	PROPN
eurjchem-1000	219	13	;	;	PUNCT
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eurjchem-1000	219	15	,	,	PUNCT
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eurjchem-1000	219	18	;	;	PUNCT
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eurjchem-1000	219	20	,	,	PUNCT
eurjchem-1000	219	21	m.	m.	PROPN
eurjchem-1000	219	22	e.	e.	PROPN
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eurjchem-1000	219	25	,	,	PUNCT
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eurjchem-1000	219	27	m.	m.	NOUN
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eurjchem-1000	219	30	a.	a.	PROPN
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eurjchem-1000	219	33	1114(1	1114(1	NUM
eurjchem-1000	219	34	)	)	PUNCT
eurjchem-1000	219	35	,	,	PUNCT
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eurjchem-1000	220	3	]	]	PUNCT
eurjchem-1000	220	4	.	.	PUNCT
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eurjchem-1000	221	2	,	,	PUNCT
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eurjchem-1000	221	5	;	;	PUNCT
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eurjchem-1000	221	11	,	,	PUNCT
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eurjchem-1000	221	17	h.	h.	PROPN
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eurjchem-1000	221	20	a.	a.	PROPN
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eurjchem-1000	221	22	,	,	PUNCT
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eurjchem-1000	221	24	,	,	PUNCT
eurjchem-1000	221	25	17‐22	17‐22	ADJ
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eurjchem-1000	222	3	]	]	PUNCT
eurjchem-1000	222	4	.	.	PUNCT
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eurjchem-1000	223	2	,	,	PUNCT
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eurjchem-1000	223	6	,	,	PUNCT
eurjchem-1000	223	7	c.	c.	PROPN
eurjchem-1000	223	8	;	;	PUNCT
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eurjchem-1000	223	10	,	,	PUNCT
eurjchem-1000	223	11	s.	s.	PROPN
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eurjchem-1000	223	17	u.	u.	PROPN
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eurjchem-1000	223	20	.	.	PROPN
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eurjchem-1000	223	22	.	.	PUNCT
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eurjchem-1000	224	2	.	.	PUNCT
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eurjchem-1000	225	2	,	,	PUNCT
eurjchem-1000	225	3	52	52	NUM
eurjchem-1000	225	4	,	,	PUNCT
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eurjchem-1000	226	3	]	]	PUNCT
eurjchem-1000	226	4	.	.	PUNCT
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eurjchem-1000	227	2	,	,	PUNCT
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eurjchem-1000	227	4	d.	d.	PROPN
eurjchem-1000	227	5	u.	u.	PROPN
eurjchem-1000	227	6	s.	s.	PROPN
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eurjchem-1000	228	9	,	,	PUNCT
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eurjchem-1000	228	11	.	.	PUNCT
eurjchem-1000	229	1	[	[	X
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eurjchem-1000	229	3	]	]	PUNCT
eurjchem-1000	229	4	.	.	PUNCT
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eurjchem-1000	230	2	,	,	PUNCT
eurjchem-1000	230	3	l.	l.	PROPN
eurjchem-1000	230	4	;	;	PUNCT
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eurjchem-1000	230	6	,	,	PUNCT
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eurjchem-1000	230	8	j.	j.	PROPN
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eurjchem-1000	230	10	.	.	PUNCT
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eurjchem-1000	230	12	.	.	PUNCT
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eurjchem-1000	231	2	.	.	PUNCT
eurjchem-1000	232	1	2003	2003	NUM
eurjchem-1000	232	2	,	,	PUNCT
eurjchem-1000	232	3	33	33	NUM
eurjchem-1000	232	4	,	,	PUNCT
eurjchem-1000	232	5	211‐217	211‐217	NUM
eurjchem-1000	232	6	.	.	PUNCT
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eurjchem-1000	233	3	]	]	PUNCT
eurjchem-1000	233	4	.	.	PUNCT
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eurjchem-1000	234	4	;	;	PUNCT
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eurjchem-1000	234	6	,	,	PUNCT
eurjchem-1000	234	7	c.	c.	PROPN
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eurjchem-1000	234	10	,	,	PUNCT
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eurjchem-1000	234	17	p.	p.	PROPN
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eurjchem-1000	234	20	.	.	PROPN
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eurjchem-1000	234	22	.	.	PUNCT
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eurjchem-1000	236	2	,	,	PUNCT
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eurjchem-1000	236	4	,	,	PUNCT
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eurjchem-1000	236	6	.	.	PUNCT
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eurjchem-1000	237	3	]	]	PUNCT
eurjchem-1000	237	4	.	.	PUNCT
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eurjchem-1000	237	6	,	,	PUNCT
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eurjchem-1000	237	8	;	;	PUNCT
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eurjchem-1000	237	10	,	,	PUNCT
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eurjchem-1000	239	2	,	,	PUNCT
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eurjchem-1000	239	6	.	.	PUNCT
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eurjchem-1000	240	4	.	.	PUNCT
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eurjchem-1000	241	6	;	;	PUNCT
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eurjchem-1000	241	10	;	;	PUNCT
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eurjchem-1000	242	4	,	,	PUNCT
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eurjchem-1000	242	6	,	,	PUNCT
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eurjchem-1000	243	8	;	;	PUNCT
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eurjchem-1000	243	10	,	,	PUNCT
eurjchem-1000	243	11	x.	x.	PROPN
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eurjchem-1000	243	14	,	,	PUNCT
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eurjchem-1000	243	18	,	,	PUNCT
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eurjchem-1000	243	22	,	,	PUNCT
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eurjchem-1000	243	26	.	.	PUNCT
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eurjchem-1000	244	2	,	,	PUNCT
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eurjchem-1000	244	5	,	,	PUNCT
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eurjchem-1000	245	3	]	]	PUNCT
eurjchem-1000	245	4	.	.	PUNCT
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eurjchem-1000	246	2	,	,	PUNCT
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eurjchem-1000	246	4	;	;	PUNCT
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eurjchem-1000	246	6	,	,	PUNCT
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eurjchem-1000	246	8	;	;	PUNCT
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eurjchem-1000	248	26	,	,	PUNCT
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eurjchem-1000	248	34	.	.	PUNCT
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eurjchem-1000	249	3	,	,	PUNCT
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eurjchem-1000	249	5	)	)	PUNCT
eurjchem-1000	249	6	,	,	PUNCT
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eurjchem-1000	250	3	]	]	PUNCT
eurjchem-1000	250	4	.	.	PUNCT
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eurjchem-1000	251	18	,	,	PUNCT
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eurjchem-1000	251	20	;	;	PUNCT
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eurjchem-1000	251	22	,	,	PUNCT
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eurjchem-1000	251	26	.	.	PUNCT
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eurjchem-1000	253	2	,	,	PUNCT
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eurjchem-1000	253	4	)	)	PUNCT
eurjchem-1000	253	5	,	,	PUNCT
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eurjchem-1000	254	4	.	.	PUNCT
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eurjchem-1000	255	2	,	,	PUNCT
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eurjchem-1000	255	6	,	,	PUNCT
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eurjchem-1000	255	10	,	,	PUNCT
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eurjchem-1000	255	14	,	,	PUNCT
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eurjchem-1000	266	10	2001	2001	NUM
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