id sid tid token lemma pos eurjchem-108 1 1 microsoft microsoft PROPN eurjchem-108 1 2 word word NOUN eurjchem-108 1 3 european_journal_of_chemistry_1_4_2010_291_293_108 european_journal_of_chemistry_1_4_2010_291_293_108 PROPN eurjchem-108 1 4 european european ADJ eurjchem-108 1 5     SPACE eurjchem-108 1 6 journal journal NOUN eurjchem-108 1 7     SPACE eurjchem-108 1 8 of of ADP eurjchem-108 1 9     SPACE eurjchem-108 1 10 chemistry chemistry NOUN eurjchem-108 1 11     SPACE eurjchem-108 1 12 1 1 NUM eurjchem-108 1 13     SPACE eurjchem-108 1 14 ( ( PUNCT eurjchem-108 1 15 4 4 NUM eurjchem-108 1 16 ) ) PUNCT eurjchem-108 1 17     SPACE eurjchem-108 1 18 ( ( PUNCT eurjchem-108 1 19 2010 2010 NUM eurjchem-108 1 20 ) ) PUNCT eurjchem-108 1 21     SPACE eurjchem-108 1 22 291‐293 291‐293 NUM eurjchem-108 1 23         SPACE eurjchem-108 1 24 european european ADJ eurjchem-108 1 25     SPACE eurjchem-108 1 26 journal journal NOUN eurjchem-108 1 27     SPACE eurjchem-108 1 28 of of ADP eurjchem-108 1 29     SPACE eurjchem-108 1 30 chemistry chemistry NOUN eurjchem-108 1 31     SPACE eurjchem-108 1 32 issn issn VERB eurjchem-108 1 33     SPACE eurjchem-108 1 34 2153‐2249 2153‐2249 NUM eurjchem-108 1 35     SPACE eurjchem-108 1 36 ( ( PUNCT eurjchem-108 1 37 print print NOUN eurjchem-108 1 38 ) ) PUNCT eurjchem-108 1 39     SPACE eurjchem-108 1 40 / / SYM eurjchem-108 1 41     SPACE eurjchem-108 1 42 issn issn VERB eurjchem-108 1 43     SPACE eurjchem-108 1 44 2153‐2257 2153‐2257 NUM eurjchem-108 1 45     SPACE eurjchem-108 1 46 ( ( PUNCT eurjchem-108 1 47 online online ADJ eurjchem-108 1 48 ) ) PUNCT eurjchem-108 1 49     SPACE eurjchem-108 1 50   NOUN eurjchem-108 1 51     SPACE eurjchem-108 1 52 2010 2010 NUM eurjchem-108 1 53     SPACE eurjchem-108 1 54 eurjchem eurjchem NOUN eurjchem-108 1 55     SPACE eurjchem-108 1 56 doi:10.5155 doi:10.5155 NOUN eurjchem-108 1 57 / / SYM eurjchem-108 1 58 eurjchem.1.4.291‐293.108 eurjchem.1.4.291‐293.108 NOUN eurjchem-108 1 59                 SPACE eurjchem-108 1 60 european european ADJ eurjchem-108 1 61     SPACE eurjchem-108 1 62 journal journal NOUN eurjchem-108 1 63     SPACE eurjchem-108 1 64 of of ADP eurjchem-108 1 65     SPACE eurjchem-108 1 66 chemistry chemistry NOUN eurjchem-108 1 67     SPACE eurjchem-108 1 68 journal journal NOUN eurjchem-108 1 69     SPACE eurjchem-108 1 70 homepage homepage NOUN eurjchem-108 1 71 : : PUNCT eurjchem-108 1 72     SPACE eurjchem-108 1 73 www.eurjchem.com www.eurjchem.com NOUN eurjchem-108 1 74                     SPACE eurjchem-108 1 75 synthesis synthesis NOUN eurjchem-108 1 76     SPACE eurjchem-108 1 77 of of ADP eurjchem-108 1 78     SPACE eurjchem-108 1 79 octahydroquinazolinone octahydroquinazolinone NOUN eurjchem-108 1 80     SPACE eurjchem-108 1 81 derivatives derivative NOUN eurjchem-108 1 82     SPACE eurjchem-108 1 83 using use VERB eurjchem-108 1 84     SPACE eurjchem-108 1 85 silica silica NOUN eurjchem-108 1 86     SPACE eurjchem-108 1 87 sulfuric sulfuric NOUN eurjchem-108 1 88     SPACE eurjchem-108 1 89 acid acid NOUN eurjchem-108 1 90     SPACE eurjchem-108 1 91 as as ADP eurjchem-108 1 92       SPACE eurjchem-108 1 93 an an DET eurjchem-108 1 94     SPACE eurjchem-108 1 95 efficient efficient ADJ eurjchem-108 1 96     SPACE eurjchem-108 1 97 catalyst catalyst NOUN eurjchem-108 1 98     SPACE eurjchem-108 1 99 akbar akbar NOUN eurjchem-108 1 100     SPACE eurjchem-108 1 101 mobinikhaledia mobinikhaledia NOUN eurjchem-108 1 102 , , PUNCT eurjchem-108 1 103 * * NOUN eurjchem-108 1 104 , , PUNCT eurjchem-108 1 105     SPACE eurjchem-108 1 106 naser naser NOUN eurjchem-108 1 107     SPACE eurjchem-108 1 108 foroughifara foroughifara PROPN eurjchem-108 1 109 , , PUNCT eurjchem-108 1 110 b b NOUN eurjchem-108 1 111     SPACE eurjchem-108 1 112 and and CCONJ eurjchem-108 1 113     SPACE eurjchem-108 1 114 homila homila NOUN eurjchem-108 1 115     SPACE eurjchem-108 1 116 khodaeia khodaeia PROPN eurjchem-108 1 117     SPACE eurjchem-108 1 118 a a DET eurjchem-108 1 119     SPACE eurjchem-108 1 120 department department NOUN eurjchem-108 1 121     SPACE eurjchem-108 1 122 of of ADP eurjchem-108 1 123     SPACE eurjchem-108 1 124 chemistry chemistry NOUN eurjchem-108 1 125 , , PUNCT eurjchem-108 1 126     SPACE eurjchem-108 1 127 arak arak PROPN eurjchem-108 1 128     SPACE eurjchem-108 1 129 university university PROPN eurjchem-108 1 130 , , PUNCT eurjchem-108 1 131     SPACE eurjchem-108 1 132 arak arak PROPN eurjchem-108 1 133 , , PUNCT eurjchem-108 1 134     SPACE eurjchem-108 1 135 ir­38156­879 ir­38156­879 NOUN eurjchem-108 1 136 , , PUNCT eurjchem-108 1 137     SPACE eurjchem-108 1 138 iran iran PROPN eurjchem-108 1 139     SPACE eurjchem-108 1 140 b b NOUN eurjchem-108 1 141     SPACE eurjchem-108 1 142 faculty faculty NOUN eurjchem-108 1 143     SPACE eurjchem-108 1 144 of of ADP eurjchem-108 1 145     SPACE eurjchem-108 1 146 chemistry chemistry NOUN eurjchem-108 1 147 , , PUNCT eurjchem-108 1 148     SPACE eurjchem-108 1 149 islamic islamic ADJ eurjchem-108 1 150     SPACE eurjchem-108 1 151 azad azad PROPN eurjchem-108 1 152     SPACE eurjchem-108 1 153 university university NOUN eurjchem-108 1 154 , , PUNCT eurjchem-108 1 155     SPACE eurjchem-108 1 156 north north NOUN eurjchem-108 1 157     SPACE eurjchem-108 1 158 tehran tehran NOUN eurjchem-108 1 159     SPACE eurjchem-108 1 160 branch branch NOUN eurjchem-108 1 161 , , PUNCT eurjchem-108 1 162     SPACE eurjchem-108 1 163 ir­1491367711 ir­1491367711 VERB eurjchem-108 1 164 , , PUNCT eurjchem-108 1 165     SPACE eurjchem-108 1 166 iran iran PROPN eurjchem-108 1 167     SPACE eurjchem-108 1 168 * * PUNCT eurjchem-108 1 169 corresponding corresponding ADJ eurjchem-108 1 170     SPACE eurjchem-108 1 171 author author NOUN eurjchem-108 1 172     SPACE eurjchem-108 1 173 at at ADP eurjchem-108 1 174 : : PUNCT eurjchem-108 1 175     SPACE eurjchem-108 1 176 department department NOUN eurjchem-108 1 177     SPACE eurjchem-108 1 178 of of ADP eurjchem-108 1 179     SPACE eurjchem-108 1 180 chemistry chemistry NOUN eurjchem-108 1 181 , , PUNCT eurjchem-108 1 182     SPACE eurjchem-108 1 183 arak arak PROPN eurjchem-108 1 184     SPACE eurjchem-108 1 185 university university PROPN eurjchem-108 1 186 , , PUNCT eurjchem-108 1 187     SPACE eurjchem-108 1 188 arak arak PROPN eurjchem-108 1 189 , , PUNCT eurjchem-108 1 190     SPACE eurjchem-108 1 191 ir­38156­879 ir­38156­879 NOUN eurjchem-108 1 192 , , PUNCT eurjchem-108 1 193     SPACE eurjchem-108 1 194 iran iran PROPN eurjchem-108 1 195 . . PUNCT eurjchem-108 1 196     SPACE eurjchem-108 2 1 tel tel PROPN eurjchem-108 2 2 . . PUNCT eurjchem-108 2 3 : : PUNCT eurjchem-108 2 4     SPACE eurjchem-108 3 1 +98.861.2774031 +98.861.2774031 ADP eurjchem-108 3 2 ; ; PUNCT eurjchem-108 3 3     SPACE eurjchem-108 3 4 fax fax NOUN eurjchem-108 3 5 : : PUNCT eurjchem-108 3 6     SPACE eurjchem-108 3 7 +98.861.2774031 +98.861.2774031 PROPN eurjchem-108 3 8 . . PUNCT eurjchem-108 3 9       SPACE eurjchem-108 3 10 e­mail e­mail NOUN eurjchem-108 3 11     SPACE eurjchem-108 3 12 address address NOUN eurjchem-108 3 13 : : PUNCT eurjchem-108 3 14     SPACE eurjchem-108 3 15 akbar_mobini@yahoo.com akbar_mobini@yahoo.com NOUN eurjchem-108 3 16     SPACE eurjchem-108 3 17 ( ( PUNCT eurjchem-108 3 18 a. a. NOUN eurjchem-108 3 19     SPACE eurjchem-108 3 20 mobinikhaledi mobinikhaledi PROPN eurjchem-108 3 21 ) ) PUNCT eurjchem-108 3 22 . . PUNCT eurjchem-108 3 23                                 SPACE eurjchem-108 4 1 article article NOUN eurjchem-108 4 2     SPACE eurjchem-108 4 3 information information NOUN eurjchem-108 4 4         SPACE eurjchem-108 4 5 abstract abstract ADJ eurjchem-108 4 6 received receive VERB eurjchem-108 4 7 : : PUNCT eurjchem-108 4 8     SPACE eurjchem-108 4 9 14 14 NUM eurjchem-108 4 10     SPACE eurjchem-108 4 11 may may AUX eurjchem-108 4 12     SPACE eurjchem-108 4 13 2010 2010 NUM eurjchem-108 4 14     SPACE eurjchem-108 4 15 received receive VERB eurjchem-108 4 16     SPACE eurjchem-108 4 17 in in ADP eurjchem-108 4 18     SPACE eurjchem-108 4 19 revised revise VERB eurjchem-108 4 20     SPACE eurjchem-108 4 21 form form NOUN eurjchem-108 4 22 : : PUNCT eurjchem-108 4 23     SPACE eurjchem-108 4 24 21 21 NUM eurjchem-108 4 25     SPACE eurjchem-108 4 26 june june PROPN eurjchem-108 4 27     SPACE eurjchem-108 4 28 2010 2010 NUM eurjchem-108 4 29     SPACE eurjchem-108 4 30 accepted accept VERB eurjchem-108 4 31 : : PUNCT eurjchem-108 4 32     SPACE eurjchem-108 4 33 14 14 NUM eurjchem-108 4 34     SPACE eurjchem-108 4 35 august august PROPN eurjchem-108 4 36     SPACE eurjchem-108 4 37 2010 2010 NUM eurjchem-108 4 38     SPACE eurjchem-108 4 39 online online NOUN eurjchem-108 4 40 : : PUNCT eurjchem-108 4 41     SPACE eurjchem-108 4 42 31 31 NUM eurjchem-108 4 43     SPACE eurjchem-108 4 44 december december PROPN eurjchem-108 4 45     SPACE eurjchem-108 4 46 2010 2010 NUM eurjchem-108 4 47     SPACE eurjchem-108 4 48 keywords keyword VERB eurjchem-108 4 49         SPACE eurjchem-108 4 50 octahydroquinazolinone octahydroquinazolinone NOUN eurjchem-108 4 51     SPACE eurjchem-108 4 52 derivatives derivative NOUN eurjchem-108 4 53     SPACE eurjchem-108 4 54 were be AUX eurjchem-108 4 55     SPACE eurjchem-108 4 56 synthesized synthesize VERB eurjchem-108 4 57     SPACE eurjchem-108 4 58 in in ADP eurjchem-108 4 59     SPACE eurjchem-108 4 60 moderate moderate ADJ eurjchem-108 4 61     SPACE eurjchem-108 4 62 to to PART eurjchem-108 4 63     SPACE eurjchem-108 4 64 high high ADJ eurjchem-108 4 65     SPACE eurjchem-108 4 66 yields yield NOUN eurjchem-108 4 67     SPACE eurjchem-108 4 68 via via ADP eurjchem-108 4 69     SPACE eurjchem-108 4 70 one‐pot one‐pot NOUN eurjchem-108 4 71     SPACE eurjchem-108 4 72 three three NUM eurjchem-108 4 73     SPACE eurjchem-108 4 74 component component NOUN eurjchem-108 4 75     SPACE eurjchem-108 4 76 biginelli biginelli NOUN eurjchem-108 4 77     SPACE eurjchem-108 4 78 reaction reaction NOUN eurjchem-108 4 79     SPACE eurjchem-108 4 80 of of ADP eurjchem-108 4 81     SPACE eurjchem-108 4 82 dimedone dimedone NOUN eurjchem-108 4 83 , , PUNCT eurjchem-108 4 84     SPACE eurjchem-108 4 85 urea urea NOUN eurjchem-108 4 86     SPACE eurjchem-108 4 87 or or CCONJ eurjchem-108 4 88     SPACE eurjchem-108 4 89 thiourea thiourea NOUN eurjchem-108 4 90     SPACE eurjchem-108 4 91 and and CCONJ eurjchem-108 4 92     SPACE eurjchem-108 4 93 corresponding corresponding ADJ eurjchem-108 4 94     SPACE eurjchem-108 4 95 aromatic aromatic NOUN eurjchem-108 4 96     SPACE eurjchem-108 4 97 aldehydes aldehyde NOUN eurjchem-108 4 98     SPACE eurjchem-108 4 99 in in ADP eurjchem-108 4 100     SPACE eurjchem-108 4 101 the the DET eurjchem-108 4 102     SPACE eurjchem-108 4 103 presence presence NOUN eurjchem-108 4 104     SPACE eurjchem-108 4 105 of of ADP eurjchem-108 4 106     SPACE eurjchem-108 4 107 silica silica NOUN eurjchem-108 4 108     SPACE eurjchem-108 4 109 sulfuric sulfuric NOUN eurjchem-108 4 110     SPACE eurjchem-108 4 111 acid acid NOUN eurjchem-108 4 112     SPACE eurjchem-108 4 113 as as ADP eurjchem-108 4 114     SPACE eurjchem-108 4 115 an an DET eurjchem-108 4 116     SPACE eurjchem-108 4 117 efficient efficient ADJ eurjchem-108 4 118     SPACE eurjchem-108 4 119 catalyst catalyst NOUN eurjchem-108 4 120 , , PUNCT eurjchem-108 4 121     SPACE eurjchem-108 4 122 in in ADP eurjchem-108 4 123     SPACE eurjchem-108 4 124 ethanol ethanol NOUN eurjchem-108 4 125     SPACE eurjchem-108 4 126 under under ADP eurjchem-108 4 127     SPACE eurjchem-108 4 128 reflux reflux NOUN eurjchem-108 4 129     SPACE eurjchem-108 4 130 conditions condition NOUN eurjchem-108 4 131 . . PUNCT eurjchem-108 4 132     SPACE eurjchem-108 5 1 this this DET eurjchem-108 5 2     SPACE eurjchem-108 5 3 protocol protocol NOUN eurjchem-108 5 4     SPACE eurjchem-108 5 5 offers offer VERB eurjchem-108 5 6     SPACE eurjchem-108 5 7 several several ADJ eurjchem-108 5 8     SPACE eurjchem-108 5 9 advantages advantage NOUN eurjchem-108 5 10     SPACE eurjchem-108 5 11 including include VERB eurjchem-108 5 12     SPACE eurjchem-108 5 13 good good ADJ eurjchem-108 5 14     SPACE eurjchem-108 5 15 yields yield NOUN eurjchem-108 5 16     SPACE eurjchem-108 5 17 of of ADP eurjchem-108 5 18     SPACE eurjchem-108 5 19 products product NOUN eurjchem-108 5 20     SPACE eurjchem-108 5 21 and and CCONJ eurjchem-108 5 22     SPACE eurjchem-108 5 23 easy easy ADJ eurjchem-108 5 24     SPACE eurjchem-108 5 25 experimental experimental ADJ eurjchem-108 5 26     SPACE eurjchem-108 5 27 work‐up work‐up ADV eurjchem-108 5 28     SPACE eurjchem-108 5 29 procedure procedure NOUN eurjchem-108 5 30 . . PUNCT eurjchem-108 5 31     SPACE eurjchem-108 6 1 quinazolinone quinazolinone NUM eurjchem-108 6 2     SPACE eurjchem-108 6 3 silica silica NOUN eurjchem-108 6 4     SPACE eurjchem-108 6 5 sulfuric sulfuric NOUN eurjchem-108 6 6     SPACE eurjchem-108 6 7 acid acid NOUN eurjchem-108 6 8     SPACE eurjchem-108 6 9 dimedone dimedone NOUN eurjchem-108 6 10     SPACE eurjchem-108 6 11 biginelli biginelli NOUN eurjchem-108 6 12     SPACE eurjchem-108 6 13 reaction reaction NOUN eurjchem-108 6 14         SPACE eurjchem-108 6 15 1 1 NUM eurjchem-108 6 16 . . PUNCT eurjchem-108 6 17     SPACE eurjchem-108 6 18 introduction introduction NOUN eurjchem-108 6 19         SPACE eurjchem-108 6 20 over over ADP eurjchem-108 6 21     SPACE eurjchem-108 6 22 the the DET eurjchem-108 6 23     SPACE eurjchem-108 6 24 years year NOUN eurjchem-108 6 25 , , PUNCT eurjchem-108 6 26     SPACE eurjchem-108 6 27 research research NOUN eurjchem-108 6 28     SPACE eurjchem-108 6 29 interest interest NOUN eurjchem-108 6 30     SPACE eurjchem-108 6 31 for for ADP eurjchem-108 6 32     SPACE eurjchem-108 6 33 the the DET eurjchem-108 6 34     SPACE eurjchem-108 6 35 synthesis synthesis NOUN eurjchem-108 6 36     SPACE eurjchem-108 6 37 of of ADP eurjchem-108 6 38     SPACE eurjchem-108 6 39 dihydro dihydro NOUN eurjchem-108 6 40     SPACE eurjchem-108 6 41 pyrimidinones pyrimidinone NOUN eurjchem-108 6 42     SPACE eurjchem-108 6 43 and and CCONJ eurjchem-108 6 44     SPACE eurjchem-108 6 45 their their PRON eurjchem-108 6 46     SPACE eurjchem-108 6 47 derivatives derivative NOUN eurjchem-108 6 48     SPACE eurjchem-108 6 49 including include VERB eurjchem-108 6 50     SPACE eurjchem-108 6 51 octahydroquinazolinone octahydroquinazolinone NOUN eurjchem-108 6 52     SPACE eurjchem-108 6 53 using use VERB eurjchem-108 6 54     SPACE eurjchem-108 6 55 multicomponents multicomponent NOUN eurjchem-108 6 56     SPACE eurjchem-108 6 57 reactions reaction NOUN eurjchem-108 6 58     SPACE eurjchem-108 6 59 has have AUX eurjchem-108 6 60     SPACE eurjchem-108 6 61 surged surge VERB eurjchem-108 6 62     SPACE eurjchem-108 6 63 rapidly rapidly ADV eurjchem-108 6 64 , , PUNCT eurjchem-108 6 65     SPACE eurjchem-108 6 66 owing owe VERB eurjchem-108 6 67     SPACE eurjchem-108 6 68 to to ADP eurjchem-108 6 69     SPACE eurjchem-108 6 70 the the DET eurjchem-108 6 71     SPACE eurjchem-108 6 72 diverse diverse ADJ eurjchem-108 6 73     SPACE eurjchem-108 6 74 pharmacological pharmacological NOUN eurjchem-108 6 75     SPACE eurjchem-108 6 76 properties property NOUN eurjchem-108 6 77     SPACE eurjchem-108 6 78 associated associate VERB eurjchem-108 6 79     SPACE eurjchem-108 6 80 with with ADP eurjchem-108 6 81     SPACE eurjchem-108 6 82 the the DET eurjchem-108 6 83     SPACE eurjchem-108 6 84 pyrimidine pyrimidine NOUN eurjchem-108 6 85     SPACE eurjchem-108 6 86 core core NOUN eurjchem-108 6 87     SPACE eurjchem-108 6 88 [ [ X eurjchem-108 6 89 1,2 1,2 NUM eurjchem-108 6 90 ] ] PUNCT eurjchem-108 6 91 . . PUNCT eurjchem-108 6 92     SPACE eurjchem-108 7 1 octahydroquinazolinone octahydroquinazolinone NOUN eurjchem-108 7 2     SPACE eurjchem-108 7 3 derivatives derivative NOUN eurjchem-108 7 4     SPACE eurjchem-108 7 5 have have AUX eurjchem-108 7 6     SPACE eurjchem-108 7 7 received receive VERB eurjchem-108 7 8     SPACE eurjchem-108 7 9 considerable considerable ADJ eurjchem-108 7 10     SPACE eurjchem-108 7 11 attention attention NOUN eurjchem-108 7 12     SPACE eurjchem-108 7 13 within within ADP eurjchem-108 7 14     SPACE eurjchem-108 7 15 recent recent ADJ eurjchem-108 7 16     SPACE eurjchem-108 7 17 years year NOUN eurjchem-108 7 18     SPACE eurjchem-108 7 19 due due ADJ eurjchem-108 7 20     SPACE eurjchem-108 7 21 to to ADP eurjchem-108 7 22     SPACE eurjchem-108 7 23 their their PRON eurjchem-108 7 24     SPACE eurjchem-108 7 25 attractive attractive ADJ eurjchem-108 7 26     SPACE eurjchem-108 7 27 pharmacological pharmacological NOUN eurjchem-108 7 28     SPACE eurjchem-108 7 29 profiles profile NOUN eurjchem-108 7 30     SPACE eurjchem-108 8 1 [ [ X eurjchem-108 8 2 2‐5 2‐5 NOUN eurjchem-108 8 3 ] ] X eurjchem-108 8 4 . . PUNCT eurjchem-108 8 5     SPACE eurjchem-108 9 1 several several ADJ eurjchem-108 9 2     SPACE eurjchem-108 9 3 methods method NOUN eurjchem-108 9 4     SPACE eurjchem-108 9 5 have have AUX eurjchem-108 9 6     SPACE eurjchem-108 9 7 been be AUX eurjchem-108 9 8     SPACE eurjchem-108 9 9 reported report VERB eurjchem-108 9 10     SPACE eurjchem-108 9 11 for for ADP eurjchem-108 9 12     SPACE eurjchem-108 9 13 the the DET eurjchem-108 9 14     SPACE eurjchem-108 9 15 synthesis synthesis NOUN eurjchem-108 9 16     SPACE eurjchem-108 9 17 of of ADP eurjchem-108 9 18     SPACE eurjchem-108 9 19 quinazolinone quinazolinone NOUN eurjchem-108 9 20     SPACE eurjchem-108 9 21 derivatives derivative NOUN eurjchem-108 9 22     SPACE eurjchem-108 10 1 [ [ X eurjchem-108 10 2 6,7 6,7 NUM eurjchem-108 10 3 ] ] PUNCT eurjchem-108 10 4 . . PUNCT eurjchem-108 10 5     SPACE eurjchem-108 11 1 these these DET eurjchem-108 11 2     SPACE eurjchem-108 11 3 methods method NOUN eurjchem-108 11 4     SPACE eurjchem-108 11 5 usually usually ADV eurjchem-108 11 6     SPACE eurjchem-108 11 7 involve involve VERB eurjchem-108 11 8     SPACE eurjchem-108 11 9 the the DET eurjchem-108 11 10     SPACE eurjchem-108 11 11 reaction reaction NOUN eurjchem-108 11 12     SPACE eurjchem-108 11 13 of of ADP eurjchem-108 11 14     SPACE eurjchem-108 11 15 an an DET eurjchem-108 11 16     SPACE eurjchem-108 11 17 aldehyde aldehyde NOUN eurjchem-108 11 18     SPACE eurjchem-108 11 19 with with ADP eurjchem-108 11 20     SPACE eurjchem-108 11 21 thionyl thionyl ADJ eurjchem-108 11 22     SPACE eurjchem-108 11 23 chloride chloride NOUN eurjchem-108 11 24     SPACE eurjchem-108 11 25 and and CCONJ eurjchem-108 11 26     SPACE eurjchem-108 11 27 pyridine pyridine NOUN eurjchem-108 11 28 , , PUNCT eurjchem-108 11 29     SPACE eurjchem-108 11 30 which which PRON eurjchem-108 11 31     SPACE eurjchem-108 11 32 is be AUX eurjchem-108 11 33     SPACE eurjchem-108 11 34 followed follow VERB eurjchem-108 11 35     SPACE eurjchem-108 11 36 in in ADP eurjchem-108 11 37     SPACE eurjchem-108 11 38 reaction reaction NOUN eurjchem-108 11 39     SPACE eurjchem-108 11 40 with with ADP eurjchem-108 11 41     SPACE eurjchem-108 11 42 2‐aminobenzylamine 2‐aminobenzylamine NOUN eurjchem-108 11 43     SPACE eurjchem-108 11 44 in in ADP eurjchem-108 11 45     SPACE eurjchem-108 11 46 different different ADJ eurjchem-108 11 47     SPACE eurjchem-108 11 48 organic organic ADJ eurjchem-108 11 49     SPACE eurjchem-108 11 50 solvents solvent NOUN eurjchem-108 11 51 . . PUNCT eurjchem-108 11 52     SPACE eurjchem-108 11 53 however however ADV eurjchem-108 11 54 , , PUNCT eurjchem-108 11 55     SPACE eurjchem-108 11 56 most most ADJ eurjchem-108 11 57     SPACE eurjchem-108 11 58 of of ADP eurjchem-108 11 59     SPACE eurjchem-108 11 60 these these DET eurjchem-108 11 61     SPACE eurjchem-108 11 62 methods method NOUN eurjchem-108 11 63     SPACE eurjchem-108 11 64 have have VERB eurjchem-108 11 65     SPACE eurjchem-108 11 66 limitations limitation NOUN eurjchem-108 11 67     SPACE eurjchem-108 11 68 including include VERB eurjchem-108 11 69     SPACE eurjchem-108 11 70 harsh harsh ADJ eurjchem-108 11 71     SPACE eurjchem-108 11 72 reaction reaction NOUN eurjchem-108 11 73     SPACE eurjchem-108 11 74 conditions condition NOUN eurjchem-108 11 75 , , PUNCT eurjchem-108 11 76     SPACE eurjchem-108 11 77 low low ADJ eurjchem-108 11 78     SPACE eurjchem-108 11 79 yields yield NOUN eurjchem-108 11 80 , , PUNCT eurjchem-108 11 81     SPACE eurjchem-108 11 82 use use NOUN eurjchem-108 11 83     SPACE eurjchem-108 11 84 of of ADP eurjchem-108 11 85     SPACE eurjchem-108 11 86 expensive expensive ADJ eurjchem-108 11 87     SPACE eurjchem-108 11 88 and and CCONJ eurjchem-108 11 89     SPACE eurjchem-108 11 90 hazardous hazardous ADJ eurjchem-108 11 91     SPACE eurjchem-108 11 92 chemicals chemical NOUN eurjchem-108 11 93 , , PUNCT eurjchem-108 11 94     SPACE eurjchem-108 11 95 and and CCONJ eurjchem-108 11 96     SPACE eurjchem-108 11 97 tedious tedious ADJ eurjchem-108 11 98     SPACE eurjchem-108 11 99 workup workup ADJ eurjchem-108 11 100     SPACE eurjchem-108 11 101 procedure procedure NOUN eurjchem-108 11 102 . . PUNCT eurjchem-108 11 103     SPACE eurjchem-108 12 1 the the DET eurjchem-108 12 2     SPACE eurjchem-108 12 3 most most ADJ eurjchem-108 12 4     SPACE eurjchem-108 12 5 general general ADJ eurjchem-108 12 6     SPACE eurjchem-108 12 7 method method NOUN eurjchem-108 12 8     SPACE eurjchem-108 12 9 for for ADP eurjchem-108 12 10     SPACE eurjchem-108 12 11 the the DET eurjchem-108 12 12     SPACE eurjchem-108 12 13 preparation preparation NOUN eurjchem-108 12 14     SPACE eurjchem-108 12 15 of of ADP eurjchem-108 12 16     SPACE eurjchem-108 12 17 octahydroquinazolinones octahydroquinazolinone NOUN eurjchem-108 12 18     SPACE eurjchem-108 12 19 involves involve VERB eurjchem-108 12 20     SPACE eurjchem-108 12 21 the the DET eurjchem-108 12 22     SPACE eurjchem-108 12 23 one‐pot one‐pot NOUN eurjchem-108 12 24     SPACE eurjchem-108 12 25 biginelli biginelli NOUN eurjchem-108 12 26     SPACE eurjchem-108 12 27 condensation condensation NOUN eurjchem-108 12 28     SPACE eurjchem-108 12 29 reaction reaction NOUN eurjchem-108 12 30     SPACE eurjchem-108 12 31 of of ADP eurjchem-108 12 32     SPACE eurjchem-108 12 33 dimedone dimedone NOUN eurjchem-108 12 34 , , PUNCT eurjchem-108 12 35     SPACE eurjchem-108 12 36 aromatic aromatic NOUN eurjchem-108 12 37     SPACE eurjchem-108 12 38 aldehydes aldehyde NOUN eurjchem-108 12 39     SPACE eurjchem-108 12 40 and and CCONJ eurjchem-108 12 41     SPACE eurjchem-108 12 42 urea urea NOUN eurjchem-108 12 43 / / SYM eurjchem-108 12 44 or or CCONJ eurjchem-108 12 45     SPACE eurjchem-108 12 46 thiourea thiourea NOUN eurjchem-108 12 47     SPACE eurjchem-108 12 48 in in ADP eurjchem-108 12 49     SPACE eurjchem-108 12 50 the the DET eurjchem-108 12 51     SPACE eurjchem-108 12 52 presence presence NOUN eurjchem-108 12 53     SPACE eurjchem-108 12 54 of of ADP eurjchem-108 12 55     SPACE eurjchem-108 12 56 a a DET eurjchem-108 12 57     SPACE eurjchem-108 12 58 lewis lewis NOUN eurjchem-108 12 59     SPACE eurjchem-108 12 60 or or CCONJ eurjchem-108 12 61     SPACE eurjchem-108 12 62 mineral mineral NOUN eurjchem-108 12 63     SPACE eurjchem-108 12 64 acids acid NOUN eurjchem-108 12 65     SPACE eurjchem-108 13 1 [ [ X eurjchem-108 13 2 5,8 5,8 NUM eurjchem-108 13 3 ] ] X eurjchem-108 13 4 . . PUNCT eurjchem-108 13 5     SPACE eurjchem-108 14 1 although although SCONJ eurjchem-108 14 2     SPACE eurjchem-108 14 3 various various ADJ eurjchem-108 14 4     SPACE eurjchem-108 14 5 lewis lewis PROPN eurjchem-108 14 6     SPACE eurjchem-108 14 7 acid acid NOUN eurjchem-108 14 8     SPACE eurjchem-108 14 9 catalysts catalyst NOUN eurjchem-108 14 10     SPACE eurjchem-108 14 11 have have AUX eurjchem-108 14 12     SPACE eurjchem-108 14 13 been be AUX eurjchem-108 14 14     SPACE eurjchem-108 14 15 used use VERB eurjchem-108 14 16     SPACE eurjchem-108 14 17 in in ADP eurjchem-108 14 18     SPACE eurjchem-108 14 19 the the DET eurjchem-108 14 20     SPACE eurjchem-108 14 21 extension extension NOUN eurjchem-108 14 22     SPACE eurjchem-108 14 23 of of ADP eurjchem-108 14 24     SPACE eurjchem-108 14 25 the the DET eurjchem-108 14 26     SPACE eurjchem-108 14 27 biginelli biginelli NOUN eurjchem-108 14 28     SPACE eurjchem-108 14 29 reaction reaction NOUN eurjchem-108 14 30 , , PUNCT eurjchem-108 14 31     SPACE eurjchem-108 14 32 they they PRON eurjchem-108 14 33     SPACE eurjchem-108 14 34 are be AUX eurjchem-108 14 35     SPACE eurjchem-108 14 36 harmful harmful ADJ eurjchem-108 14 37 , , PUNCT eurjchem-108 14 38     SPACE eurjchem-108 14 39 expensive expensive ADJ eurjchem-108 14 40     SPACE eurjchem-108 14 41 and and CCONJ eurjchem-108 14 42     SPACE eurjchem-108 14 43 difficult difficult ADJ eurjchem-108 14 44     SPACE eurjchem-108 14 45 to to PART eurjchem-108 14 46     SPACE eurjchem-108 14 47 handle handle VERB eurjchem-108 14 48     SPACE eurjchem-108 14 49 [ [ X eurjchem-108 14 50 9‐13 9‐13 NUM eurjchem-108 14 51 ] ] X eurjchem-108 14 52 . . PUNCT eurjchem-108 14 53     SPACE eurjchem-108 14 54 consequently consequently ADV eurjchem-108 14 55 , , PUNCT eurjchem-108 14 56     SPACE eurjchem-108 14 57 the the DET eurjchem-108 14 58     SPACE eurjchem-108 14 59 introduction introduction NOUN eurjchem-108 14 60     SPACE eurjchem-108 14 61 of of ADP eurjchem-108 14 62     SPACE eurjchem-108 14 63 new new ADJ eurjchem-108 14 64     SPACE eurjchem-108 14 65 methods method NOUN eurjchem-108 14 66     SPACE eurjchem-108 14 67 and and CCONJ eurjchem-108 14 68     SPACE eurjchem-108 14 69 /or /or AUX eurjchem-108 14 70     SPACE eurjchem-108 14 71 further further ADJ eurjchem-108 14 72     SPACE eurjchem-108 14 73 work work VERB eurjchem-108 14 74     SPACE eurjchem-108 14 75 on on ADP eurjchem-108 14 76     SPACE eurjchem-108 14 77 technical technical ADJ eurjchem-108 14 78     SPACE eurjchem-108 14 79 improvements improvement NOUN eurjchem-108 14 80     SPACE eurjchem-108 14 81 to to PART eurjchem-108 14 82     SPACE eurjchem-108 14 83 overcome overcome VERB eurjchem-108 14 84     SPACE eurjchem-108 14 85 these these DET eurjchem-108 14 86     SPACE eurjchem-108 14 87 limitations limitation NOUN eurjchem-108 14 88     SPACE eurjchem-108 14 89 is be AUX eurjchem-108 14 90     SPACE eurjchem-108 14 91 still still ADV eurjchem-108 14 92     SPACE eurjchem-108 14 93 needed need VERB eurjchem-108 14 94 . . PUNCT eurjchem-108 14 95     SPACE eurjchem-108 14 96 recently recently ADV eurjchem-108 14 97 , , PUNCT eurjchem-108 14 98     SPACE eurjchem-108 14 99 the the DET eurjchem-108 14 100     SPACE eurjchem-108 14 101 use use NOUN eurjchem-108 14 102     SPACE eurjchem-108 14 103 of of ADP eurjchem-108 14 104     SPACE eurjchem-108 14 105 silica silica NOUN eurjchem-108 14 106     SPACE eurjchem-108 14 107 sulfuric sulfuric NOUN eurjchem-108 14 108     SPACE eurjchem-108 14 109 acid acid NOUN eurjchem-108 14 110     SPACE eurjchem-108 14 111 ( ( PUNCT eurjchem-108 14 112 ssa ssa NOUN eurjchem-108 14 113 ) ) PUNCT eurjchem-108 14 114     SPACE eurjchem-108 14 115 as as ADP eurjchem-108 14 116     SPACE eurjchem-108 14 117 a a DET eurjchem-108 14 118     SPACE eurjchem-108 14 119 versatile versatile ADJ eurjchem-108 14 120     SPACE eurjchem-108 14 121 heterogeneous heterogeneous ADJ eurjchem-108 14 122     SPACE eurjchem-108 14 123 stable stable ADJ eurjchem-108 14 124     SPACE eurjchem-108 14 125 acidic acidic ADJ eurjchem-108 14 126     SPACE eurjchem-108 14 127 catalyst catalyst NOUN eurjchem-108 14 128     SPACE eurjchem-108 14 129 in in ADP eurjchem-108 14 130     SPACE eurjchem-108 14 131 organic organic ADJ eurjchem-108 14 132     SPACE eurjchem-108 14 133 synthesis synthesis NOUN eurjchem-108 14 134     SPACE eurjchem-108 14 135 has have AUX eurjchem-108 14 136     SPACE eurjchem-108 14 137 been be AUX eurjchem-108 14 138     SPACE eurjchem-108 14 139 reported report VERB eurjchem-108 14 140     SPACE eurjchem-108 14 141 [ [ X eurjchem-108 14 142 14‐18 14‐18 NUM eurjchem-108 14 143 ] ] PUNCT eurjchem-108 14 144 . . PUNCT eurjchem-108 14 145     SPACE eurjchem-108 14 146 some some DET eurjchem-108 14 147     SPACE eurjchem-108 14 148 advantages advantage NOUN eurjchem-108 14 149     SPACE eurjchem-108 14 150 of of ADP eurjchem-108 14 151     SPACE eurjchem-108 14 152 this this DET eurjchem-108 14 153     SPACE eurjchem-108 14 154 catalyst catalyst NOUN eurjchem-108 14 155     SPACE eurjchem-108 14 156 are be AUX eurjchem-108 14 157     SPACE eurjchem-108 14 158 inexpensive inexpensive ADJ eurjchem-108 14 159 , , PUNCT eurjchem-108 14 160     SPACE eurjchem-108 14 161 easy easy ADJ eurjchem-108 14 162     SPACE eurjchem-108 14 163 to to PART eurjchem-108 14 164     SPACE eurjchem-108 14 165 prepare prepare VERB eurjchem-108 14 166     SPACE eurjchem-108 14 167 and and CCONJ eurjchem-108 14 168     SPACE eurjchem-108 14 169 insoluble insoluble ADJ eurjchem-108 14 170     SPACE eurjchem-108 14 171 in in ADP eurjchem-108 14 172     SPACE eurjchem-108 14 173 most most ADJ eurjchem-108 14 174     SPACE eurjchem-108 14 175 organic organic ADJ eurjchem-108 14 176     SPACE eurjchem-108 14 177 solvents solvent NOUN eurjchem-108 14 178 , , PUNCT eurjchem-108 14 179     SPACE eurjchem-108 14 180 which which PRON eurjchem-108 14 181     SPACE eurjchem-108 14 182 could could AUX eurjchem-108 14 183     SPACE eurjchem-108 14 184 be be AUX eurjchem-108 14 185     SPACE eurjchem-108 14 186 recycled recycle VERB eurjchem-108 14 187     SPACE eurjchem-108 14 188 during during ADP eurjchem-108 14 189     SPACE eurjchem-108 14 190 work‐up work‐up PROPN eurjchem-108 14 191 . . PUNCT eurjchem-108 14 192     SPACE eurjchem-108 14 193 in in ADP eurjchem-108 14 194     SPACE eurjchem-108 14 195 view view NOUN eurjchem-108 14 196     SPACE eurjchem-108 14 197 of of ADP eurjchem-108 14 198     SPACE eurjchem-108 14 199 these these DET eurjchem-108 14 200     SPACE eurjchem-108 14 201 observations observation NOUN eurjchem-108 14 202     SPACE eurjchem-108 14 203 and and CCONJ eurjchem-108 14 204     SPACE eurjchem-108 14 205 also also ADV eurjchem-108 14 206     SPACE eurjchem-108 14 207 due due ADJ eurjchem-108 14 208     SPACE eurjchem-108 14 209 to to ADP eurjchem-108 14 210     SPACE eurjchem-108 14 211 our our PRON eurjchem-108 14 212     SPACE eurjchem-108 14 213 interest interest NOUN eurjchem-108 14 214     SPACE eurjchem-108 14 215 in in ADP eurjchem-108 14 216     SPACE eurjchem-108 14 217 the the DET eurjchem-108 14 218     SPACE eurjchem-108 14 219 extension extension NOUN eurjchem-108 14 220     SPACE eurjchem-108 14 221 of of ADP eurjchem-108 14 222     SPACE eurjchem-108 14 223 the the DET eurjchem-108 14 224     SPACE eurjchem-108 14 225 biginelli biginelli NOUN eurjchem-108 14 226     SPACE eurjchem-108 14 227 reaction reaction NOUN eurjchem-108 14 228     SPACE eurjchem-108 15 1 [ [ X eurjchem-108 15 2 9,10,20,21 9,10,20,21 NUM eurjchem-108 15 3 ] ] X eurjchem-108 15 4 , , PUNCT eurjchem-108 15 5     SPACE eurjchem-108 15 6 we we PRON eurjchem-108 15 7     SPACE eurjchem-108 15 8 wish wish VERB eurjchem-108 15 9     SPACE eurjchem-108 15 10 to to PART eurjchem-108 15 11     SPACE eurjchem-108 15 12 report report VERB eurjchem-108 15 13     SPACE eurjchem-108 15 14 a a DET eurjchem-108 15 15     SPACE eurjchem-108 15 16 simple simple ADJ eurjchem-108 15 17 , , PUNCT eurjchem-108 15 18     SPACE eurjchem-108 15 19 cheap cheap ADJ eurjchem-108 15 20     SPACE eurjchem-108 15 21 and and CCONJ eurjchem-108 15 22     SPACE eurjchem-108 15 23 convenient convenient ADJ eurjchem-108 15 24     SPACE eurjchem-108 15 25 method method NOUN eurjchem-108 15 26     SPACE eurjchem-108 15 27 for for ADP eurjchem-108 15 28     SPACE eurjchem-108 15 29 the the DET eurjchem-108 15 30     SPACE eurjchem-108 15 31 synthesis synthesis NOUN eurjchem-108 15 32     SPACE eurjchem-108 15 33 of of ADP eurjchem-108 15 34     SPACE eurjchem-108 15 35 octahydroquinazolinone octahydroquinazolinone NOUN eurjchem-108 15 36     SPACE eurjchem-108 15 37 using use VERB eurjchem-108 15 38     SPACE eurjchem-108 15 39 silica silica NOUN eurjchem-108 15 40     SPACE eurjchem-108 15 41 sulfuric sulfuric NOUN eurjchem-108 15 42     SPACE eurjchem-108 15 43 acid acid NOUN eurjchem-108 15 44     SPACE eurjchem-108 15 45 ( ( PUNCT eurjchem-108 15 46 ssa ssa NOUN eurjchem-108 15 47 ) ) PUNCT eurjchem-108 15 48     SPACE eurjchem-108 15 49 as as ADP eurjchem-108 15 50     SPACE eurjchem-108 15 51 a a DET eurjchem-108 15 52     SPACE eurjchem-108 15 53 catalyst catalyst NOUN eurjchem-108 15 54 . . PUNCT eurjchem-108 15 55         SPACE eurjchem-108 16 1 2 2 NUM eurjchem-108 16 2 . . PUNCT eurjchem-108 16 3     SPACE eurjchem-108 16 4 experimental experimental ADJ eurjchem-108 16 5         SPACE eurjchem-108 16 6 2.1 2.1 NUM eurjchem-108 16 7 . . PUNCT eurjchem-108 16 8     SPACE eurjchem-108 16 9 instrumentation instrumentation NOUN eurjchem-108 16 10         SPACE eurjchem-108 16 11 all all PRON eurjchem-108 16 12     SPACE eurjchem-108 16 13 used use VERB eurjchem-108 16 14     SPACE eurjchem-108 16 15 chemicals chemical NOUN eurjchem-108 16 16     SPACE eurjchem-108 16 17 were be AUX eurjchem-108 16 18     SPACE eurjchem-108 16 19 purchased purchase VERB eurjchem-108 16 20     SPACE eurjchem-108 16 21 from from ADP eurjchem-108 16 22     SPACE eurjchem-108 16 23 merck merck NOUN eurjchem-108 16 24     SPACE eurjchem-108 16 25 or or CCONJ eurjchem-108 16 26     SPACE eurjchem-108 16 27 fluka fluka VERB eurjchem-108 16 28     SPACE eurjchem-108 16 29 company company NOUN eurjchem-108 16 30 . . PUNCT eurjchem-108 16 31     SPACE eurjchem-108 16 32 melting melt VERB eurjchem-108 16 33     SPACE eurjchem-108 16 34 points point NOUN eurjchem-108 16 35     SPACE eurjchem-108 16 36 were be AUX eurjchem-108 16 37     SPACE eurjchem-108 16 38 determined determine VERB eurjchem-108 16 39     SPACE eurjchem-108 16 40 on on ADP eurjchem-108 16 41     SPACE eurjchem-108 16 42 an an DET eurjchem-108 16 43     SPACE eurjchem-108 16 44 electrothermal electrothermal ADJ eurjchem-108 16 45     SPACE eurjchem-108 16 46 digital digital ADJ eurjchem-108 16 47     SPACE eurjchem-108 16 48 melting melting NOUN eurjchem-108 16 49     SPACE eurjchem-108 16 50 point point NOUN eurjchem-108 16 51     SPACE eurjchem-108 16 52 apparatus apparatus NOUN eurjchem-108 16 53 . . PUNCT eurjchem-108 16 54     SPACE eurjchem-108 17 1 the the DET eurjchem-108 17 2     SPACE eurjchem-108 17 3 ir ir PROPN eurjchem-108 17 4     SPACE eurjchem-108 17 5 spectra spectra NOUN eurjchem-108 17 6     SPACE eurjchem-108 17 7 were be AUX eurjchem-108 17 8     SPACE eurjchem-108 17 9 recorded record VERB eurjchem-108 17 10     SPACE eurjchem-108 17 11 on on ADP eurjchem-108 17 12     SPACE eurjchem-108 17 13 unicom unicom NOUN eurjchem-108 17 14     SPACE eurjchem-108 17 15 galaxy galaxy PROPN eurjchem-108 17 16     SPACE eurjchem-108 17 17 series series NOUN eurjchem-108 17 18     SPACE eurjchem-108 17 19 ft‐ir ft‐ir NOUN eurjchem-108 17 20     SPACE eurjchem-108 17 21 5000 5000 NUM eurjchem-108 17 22     SPACE eurjchem-108 17 23 spectrometer spectrometer NOUN eurjchem-108 17 24 . . PUNCT eurjchem-108 17 25     SPACE eurjchem-108 18 1 nmr nmr NOUN eurjchem-108 18 2     SPACE eurjchem-108 18 3 spectra spectra NOUN eurjchem-108 18 4     SPACE eurjchem-108 18 5 were be AUX eurjchem-108 18 6     SPACE eurjchem-108 18 7 recorded record VERB eurjchem-108 18 8     SPACE eurjchem-108 18 9 on on ADP eurjchem-108 18 10     SPACE eurjchem-108 18 11 a a DET eurjchem-108 18 12     SPACE eurjchem-108 18 13 bruker bruker NOUN eurjchem-108 18 14     SPACE eurjchem-108 18 15 avance avance PROPN eurjchem-108 18 16     SPACE eurjchem-108 18 17 ( ( PUNCT eurjchem-108 18 18 300 300 NUM eurjchem-108 18 19     SPACE eurjchem-108 18 20 mhz mhz NOUN eurjchem-108 18 21 ) ) PUNCT eurjchem-108 18 22     SPACE eurjchem-108 18 23 spectrometer spectrometer NOUN eurjchem-108 18 24 . . PUNCT eurjchem-108 18 25     SPACE eurjchem-108 19 1 chemical chemical NOUN eurjchem-108 19 2     SPACE eurjchem-108 19 3 shifts shift NOUN eurjchem-108 19 4     SPACE eurjchem-108 19 5 ( ( PUNCT eurjchem-108 19 6 ppm ppm NOUN eurjchem-108 19 7 ) ) PUNCT eurjchem-108 19 8     SPACE eurjchem-108 19 9 were be AUX eurjchem-108 19 10     SPACE eurjchem-108 19 11 referenced reference VERB eurjchem-108 19 12     SPACE eurjchem-108 19 13 to to ADP eurjchem-108 19 14     SPACE eurjchem-108 19 15 the the DET eurjchem-108 19 16     SPACE eurjchem-108 19 17 internal internal ADJ eurjchem-108 19 18     SPACE eurjchem-108 19 19 standard standard NOUN eurjchem-108 19 20     SPACE eurjchem-108 19 21 tetramethylsilane tetramethylsilane NOUN eurjchem-108 19 22     SPACE eurjchem-108 19 23 ( ( PUNCT eurjchem-108 19 24 tms tms PROPN eurjchem-108 19 25 ) ) PUNCT eurjchem-108 19 26 . . PUNCT eurjchem-108 19 27     SPACE eurjchem-108 20 1 microanalyses microanalysis NOUN eurjchem-108 20 2     SPACE eurjchem-108 20 3 were be AUX eurjchem-108 20 4     SPACE eurjchem-108 20 5 performed perform VERB eurjchem-108 20 6     SPACE eurjchem-108 20 7 by by ADP eurjchem-108 20 8     SPACE eurjchem-108 20 9 the the DET eurjchem-108 20 10     SPACE eurjchem-108 20 11 elemental elemental NOUN eurjchem-108 20 12     SPACE eurjchem-108 20 13 analyzer analyzer NOUN eurjchem-108 20 14     SPACE eurjchem-108 20 15 ( ( PUNCT eurjchem-108 20 16 elemental elemental ADJ eurjchem-108 20 17 , , PUNCT eurjchem-108 20 18     SPACE eurjchem-108 20 19 vario vario PROPN eurjchem-108 20 20     SPACE eurjchem-108 20 21 el el PROPN eurjchem-108 20 22     SPACE eurjchem-108 20 23 iii iii NOUN eurjchem-108 20 24 ) ) PUNCT eurjchem-108 20 25     SPACE eurjchem-108 20 26 at at ADP eurjchem-108 20 27     SPACE eurjchem-108 20 28 the the DET eurjchem-108 20 29     SPACE eurjchem-108 20 30 arak arak PROPN eurjchem-108 20 31     SPACE eurjchem-108 20 32 university university NOUN eurjchem-108 20 33 . . PUNCT eurjchem-108 20 34     SPACE eurjchem-108 21 1 the the DET eurjchem-108 21 2     SPACE eurjchem-108 21 3 micro‐ micro‐ NOUN eurjchem-108 21 4 analyses analyse VERB eurjchem-108 21 5     SPACE eurjchem-108 21 6 results result NOUN eurjchem-108 21 7     SPACE eurjchem-108 21 8 were be AUX eurjchem-108 21 9     SPACE eurjchem-108 21 10 agreed agree VERB eurjchem-108 21 11     SPACE eurjchem-108 21 12 favorably favorably ADV eurjchem-108 21 13     SPACE eurjchem-108 21 14 with with ADP eurjchem-108 21 15     SPACE eurjchem-108 21 16 the the DET eurjchem-108 21 17     SPACE eurjchem-108 21 18 calculated calculate VERB eurjchem-108 21 19     SPACE eurjchem-108 21 20 values value NOUN eurjchem-108 21 21 . . PUNCT eurjchem-108 21 22     SPACE eurjchem-108 22 1 reactions reaction NOUN eurjchem-108 22 2     SPACE eurjchem-108 22 3 were be AUX eurjchem-108 22 4     SPACE eurjchem-108 22 5 monitored monitor VERB eurjchem-108 22 6     SPACE eurjchem-108 22 7 by by ADP eurjchem-108 22 8     SPACE eurjchem-108 22 9 thin thin ADJ eurjchem-108 22 10     SPACE eurjchem-108 22 11 layer layer NOUN eurjchem-108 22 12     SPACE eurjchem-108 22 13 chroma‐ chroma‐ NUM eurjchem-108 22 14 tography tography NOUN eurjchem-108 22 15     SPACE eurjchem-108 22 16 using use VERB eurjchem-108 22 17     SPACE eurjchem-108 22 18 silica silica NOUN eurjchem-108 22 19     SPACE eurjchem-108 22 20 gel gel NOUN eurjchem-108 22 21     SPACE eurjchem-108 22 22 f254 f254 PROPN eurjchem-108 22 23     SPACE eurjchem-108 22 24 aluminum aluminum NOUN eurjchem-108 22 25     SPACE eurjchem-108 22 26 sheets sheet NOUN eurjchem-108 22 27     SPACE eurjchem-108 22 28 ( ( PUNCT eurjchem-108 22 29 merck merck PROPN eurjchem-108 22 30 ) ) PUNCT eurjchem-108 22 31 . . PUNCT eurjchem-108 22 32     SPACE eurjchem-108 22 33 silica silica NOUN eurjchem-108 22 34     SPACE eurjchem-108 22 35 sulfuric sulfuric NOUN eurjchem-108 22 36     SPACE eurjchem-108 22 37 acid acid NOUN eurjchem-108 22 38     SPACE eurjchem-108 22 39 ( ( PUNCT eurjchem-108 22 40 ssa ssa NOUN eurjchem-108 22 41 ) ) PUNCT eurjchem-108 22 42     SPACE eurjchem-108 22 43 was be AUX eurjchem-108 22 44     SPACE eurjchem-108 22 45 prepared prepare VERB eurjchem-108 22 46     SPACE eurjchem-108 22 47 according accord VERB eurjchem-108 22 48     SPACE eurjchem-108 22 49 to to ADP eurjchem-108 22 50     SPACE eurjchem-108 22 51 the the DET eurjchem-108 22 52     SPACE eurjchem-108 22 53 method method NOUN eurjchem-108 22 54     SPACE eurjchem-108 22 55 described describe VERB eurjchem-108 22 56     SPACE eurjchem-108 22 57 by by ADP eurjchem-108 22 58     SPACE eurjchem-108 22 59 literature literature NOUN eurjchem-108 22 60     SPACE eurjchem-108 23 1 [ [ X eurjchem-108 23 2 14 14 NUM eurjchem-108 23 3 ] ] PUNCT eurjchem-108 23 4 . . PUNCT eurjchem-108 23 5         SPACE eurjchem-108 24 1 2.2 2.2 NUM eurjchem-108 24 2 . . PUNCT eurjchem-108 24 3     SPACE eurjchem-108 24 4 general general ADJ eurjchem-108 24 5     SPACE eurjchem-108 24 6 procedure procedure NOUN eurjchem-108 24 7     SPACE eurjchem-108 24 8 for for ADP eurjchem-108 24 9     SPACE eurjchem-108 24 10 preparation preparation NOUN eurjchem-108 24 11     SPACE eurjchem-108 24 12 4a­o 4a­o PROPN eurjchem-108 24 13         SPACE eurjchem-108 24 14 a a DET eurjchem-108 24 15     SPACE eurjchem-108 24 16 solution solution NOUN eurjchem-108 24 17     SPACE eurjchem-108 24 18 of of ADP eurjchem-108 24 19     SPACE eurjchem-108 24 20 benzaldhyde benzaldhyde NOUN eurjchem-108 24 21     SPACE eurjchem-108 24 22 ( ( PUNCT eurjchem-108 24 23 2 2 NUM eurjchem-108 24 24     SPACE eurjchem-108 24 25 mmol mmol NOUN eurjchem-108 24 26 ) ) PUNCT eurjchem-108 24 27 , , PUNCT eurjchem-108 24 28     SPACE eurjchem-108 24 29 dimedone dimedone NOUN eurjchem-108 24 30     SPACE eurjchem-108 24 31 ( ( PUNCT eurjchem-108 24 32 2 2 NUM eurjchem-108 24 33     SPACE eurjchem-108 24 34 mmol mmol NOUN eurjchem-108 24 35 ) ) PUNCT eurjchem-108 24 36     SPACE eurjchem-108 24 37 and and CCONJ eurjchem-108 24 38     SPACE eurjchem-108 24 39 urea urea NOUN eurjchem-108 24 40     SPACE eurjchem-108 24 41 or or CCONJ eurjchem-108 24 42     SPACE eurjchem-108 24 43 thiourea thiourea NOUN eurjchem-108 24 44     SPACE eurjchem-108 24 45 ( ( PUNCT eurjchem-108 24 46 4 4 NUM eurjchem-108 24 47     SPACE eurjchem-108 24 48 mmol mmol NOUN eurjchem-108 24 49 ) ) PUNCT eurjchem-108 24 50     SPACE eurjchem-108 24 51 in in ADP eurjchem-108 24 52     SPACE eurjchem-108 24 53 ethanol ethanol NOUN eurjchem-108 24 54     SPACE eurjchem-108 24 55 ( ( PUNCT eurjchem-108 24 56 5 5 NUM eurjchem-108 24 57     SPACE eurjchem-108 24 58 ml ml NOUN eurjchem-108 24 59 ) ) PUNCT eurjchem-108 24 60     SPACE eurjchem-108 24 61 was be AUX eurjchem-108 24 62     SPACE eurjchem-108 24 63 added add VERB eurjchem-108 24 64     SPACE eurjchem-108 24 65 silica silica NOUN eurjchem-108 24 66     SPACE eurjchem-108 24 67 sulfuric sulfuric NOUN eurjchem-108 24 68     SPACE eurjchem-108 24 69 acid acid NOUN eurjchem-108 24 70     SPACE eurjchem-108 24 71 ( ( PUNCT eurjchem-108 24 72 0.5 0.5 NUM eurjchem-108 24 73     SPACE eurjchem-108 24 74 g g NOUN eurjchem-108 24 75 ) ) PUNCT eurjchem-108 24 76     SPACE eurjchem-108 24 77 ( ( PUNCT eurjchem-108 24 78 scheme scheme NOUN eurjchem-108 24 79     SPACE eurjchem-108 24 80 1 1 NUM eurjchem-108 24 81 ) ) PUNCT eurjchem-108 24 82 . . PUNCT eurjchem-108 24 83                       SPACE eurjchem-108 25 1 292 292 NUM eurjchem-108 25 2     SPACE eurjchem-108 25 3 mobinikhaledi mobinikhaledi PROPN eurjchem-108 25 4     SPACE eurjchem-108 25 5 et et PROPN eurjchem-108 25 6     SPACE eurjchem-108 25 7 al al PROPN eurjchem-108 25 8 . . PROPN eurjchem-108 25 9     SPACE eurjchem-108 25 10 / / SYM eurjchem-108 25 11     SPACE eurjchem-108 25 12 european european ADJ eurjchem-108 25 13     SPACE eurjchem-108 25 14 journal journal NOUN eurjchem-108 25 15     SPACE eurjchem-108 25 16 of of ADP eurjchem-108 25 17     SPACE eurjchem-108 25 18 chemistry chemistry NOUN eurjchem-108 25 19     SPACE eurjchem-108 25 20 1 1 NUM eurjchem-108 25 21     SPACE eurjchem-108 25 22 ( ( PUNCT eurjchem-108 25 23 4 4 NUM eurjchem-108 25 24 ) ) PUNCT eurjchem-108 25 25     SPACE eurjchem-108 25 26 ( ( PUNCT eurjchem-108 25 27 2010 2010 NUM eurjchem-108 25 28 ) ) PUNCT eurjchem-108 25 29     SPACE eurjchem-108 25 30 291­293 291­293 NUM eurjchem-108 25 31         SPACE eurjchem-108 25 32 scheme scheme NOUN eurjchem-108 25 33     SPACE eurjchem-108 25 34 1 1 NUM eurjchem-108 25 35             SPACE eurjchem-108 25 36 the the DET eurjchem-108 25 37     SPACE eurjchem-108 25 38 reaction reaction NOUN eurjchem-108 25 39     SPACE eurjchem-108 25 40 mixture mixture NOUN eurjchem-108 25 41     SPACE eurjchem-108 25 42 was be AUX eurjchem-108 25 43     SPACE eurjchem-108 25 44 refluxed refluxe VERB eurjchem-108 25 45     SPACE eurjchem-108 25 46 for for ADP eurjchem-108 25 47     SPACE eurjchem-108 25 48 desired desire VERB eurjchem-108 25 49     SPACE eurjchem-108 25 50 time time NOUN eurjchem-108 25 51     SPACE eurjchem-108 25 52 and and CCONJ eurjchem-108 25 53     SPACE eurjchem-108 25 54 then then ADV eurjchem-108 25 55     SPACE eurjchem-108 25 56 cooled cool VERB eurjchem-108 25 57     SPACE eurjchem-108 25 58 to to ADP eurjchem-108 25 59     SPACE eurjchem-108 25 60 room room NOUN eurjchem-108 25 61     SPACE eurjchem-108 25 62 temperature temperature NOUN eurjchem-108 25 63 . . PUNCT eurjchem-108 25 64     SPACE eurjchem-108 26 1 the the DET eurjchem-108 26 2     SPACE eurjchem-108 26 3 solvent solvent NOUN eurjchem-108 26 4     SPACE eurjchem-108 26 5 was be AUX eurjchem-108 26 6     SPACE eurjchem-108 26 7 removed remove VERB eurjchem-108 26 8     SPACE eurjchem-108 26 9 and and CCONJ eurjchem-108 26 10     SPACE eurjchem-108 26 11 the the DET eurjchem-108 26 12     SPACE eurjchem-108 26 13 solid solid ADJ eurjchem-108 26 14     SPACE eurjchem-108 26 15 mixture mixture NOUN eurjchem-108 26 16     SPACE eurjchem-108 26 17 washed wash VERB eurjchem-108 26 18     SPACE eurjchem-108 26 19 with with ADP eurjchem-108 26 20     SPACE eurjchem-108 26 21 cold cold ADJ eurjchem-108 26 22     SPACE eurjchem-108 26 23 water water NOUN eurjchem-108 26 24     SPACE eurjchem-108 26 25 ( ( PUNCT eurjchem-108 26 26 50 50 NUM eurjchem-108 26 27     SPACE eurjchem-108 26 28 ml ml NOUN eurjchem-108 26 29 ) ) PUNCT eurjchem-108 26 30     SPACE eurjchem-108 26 31 to to PART eurjchem-108 26 32     SPACE eurjchem-108 26 33 remove remove VERB eurjchem-108 26 34     SPACE eurjchem-108 26 35 the the DET eurjchem-108 26 36     SPACE eurjchem-108 26 37 excess excess NOUN eurjchem-108 26 38     SPACE eurjchem-108 26 39 of of ADP eurjchem-108 26 40     SPACE eurjchem-108 26 41 urea urea NOUN eurjchem-108 26 42     SPACE eurjchem-108 26 43 or or CCONJ eurjchem-108 26 44     SPACE eurjchem-108 26 45 thiourea thiourea NOUN eurjchem-108 26 46     SPACE eurjchem-108 26 47 and and CCONJ eurjchem-108 26 48     SPACE eurjchem-108 26 49 then then ADV eurjchem-108 26 50     SPACE eurjchem-108 26 51 filtered filter VERB eurjchem-108 26 52 . . PUNCT eurjchem-108 26 53     SPACE eurjchem-108 27 1 the the DET eurjchem-108 27 2     SPACE eurjchem-108 27 3 remaining remain VERB eurjchem-108 27 4     SPACE eurjchem-108 27 5 solid solid ADJ eurjchem-108 27 6     SPACE eurjchem-108 27 7 material material NOUN eurjchem-108 27 8     SPACE eurjchem-108 27 9 was be AUX eurjchem-108 27 10     SPACE eurjchem-108 27 11 washed wash VERB eurjchem-108 27 12     SPACE eurjchem-108 27 13 with with ADP eurjchem-108 27 14     SPACE eurjchem-108 27 15 hot hot ADJ eurjchem-108 27 16     SPACE eurjchem-108 27 17 ethylacetate ethylacetate VERB eurjchem-108 27 18     SPACE eurjchem-108 27 19 ( ( PUNCT eurjchem-108 27 20 30 30 NUM eurjchem-108 27 21     SPACE eurjchem-108 27 22 ml ml NOUN eurjchem-108 27 23 ) ) PUNCT eurjchem-108 27 24     SPACE eurjchem-108 27 25 and and CCONJ eurjchem-108 27 26     SPACE eurjchem-108 27 27 filtered filter VERB eurjchem-108 27 28 . . PUNCT eurjchem-108 27 29     SPACE eurjchem-108 28 1 the the DET eurjchem-108 28 2     SPACE eurjchem-108 28 3 filtrate filtrate NOUN eurjchem-108 28 4     SPACE eurjchem-108 28 5 was be AUX eurjchem-108 28 6     SPACE eurjchem-108 28 7 concentrated concentrate VERB eurjchem-108 28 8 , , PUNCT eurjchem-108 28 9     SPACE eurjchem-108 28 10 the the DET eurjchem-108 28 11     SPACE eurjchem-108 28 12 solid solid ADJ eurjchem-108 28 13     SPACE eurjchem-108 28 14 product product NOUN eurjchem-108 28 15     SPACE eurjchem-108 28 16 was be AUX eurjchem-108 28 17     SPACE eurjchem-108 28 18 separated separate VERB eurjchem-108 28 19 , , PUNCT eurjchem-108 28 20     SPACE eurjchem-108 28 21 air air NOUN eurjchem-108 28 22     SPACE eurjchem-108 28 23 dried dry VERB eurjchem-108 28 24 , , PUNCT eurjchem-108 28 25     SPACE eurjchem-108 28 26 and and CCONJ eurjchem-108 28 27     SPACE eurjchem-108 28 28 recrystallized recrystallize VERB eurjchem-108 28 29     SPACE eurjchem-108 28 30 from from ADP eurjchem-108 28 31     SPACE eurjchem-108 28 32 ethanol ethanol NOUN eurjchem-108 28 33     SPACE eurjchem-108 28 34 to to PART eurjchem-108 28 35     SPACE eurjchem-108 28 36 give give VERB eurjchem-108 28 37     SPACE eurjchem-108 28 38 the the DET eurjchem-108 28 39     SPACE eurjchem-108 28 40 pure pure ADJ eurjchem-108 28 41     SPACE eurjchem-108 28 42 product product NOUN eurjchem-108 28 43 . . PUNCT eurjchem-108 28 44     SPACE eurjchem-108 29 1 4‐phenyl‐7,7‐dimethyl‐1,2,3,4,5,6,7,8‐octahydroquinazo 4‐phenyl‐7,7‐dimethyl‐1,2,3,4,5,6,7,8‐octahydroquinazo PRON eurjchem-108 29 2     SPACE eurjchem-108 29 3 line‐2,5‐dione line‐2,5‐dione NOUN eurjchem-108 29 4     SPACE eurjchem-108 29 5 ( ( PUNCT eurjchem-108 29 6 4a 4a NUM eurjchem-108 29 7 ): ): PUNCT eurjchem-108 29 8     SPACE eurjchem-108 29 9 ir ir NOUN eurjchem-108 29 10     SPACE eurjchem-108 29 11 ( ( PUNCT eurjchem-108 29 12 kbr kbr PROPN eurjchem-108 29 13 , , PUNCT eurjchem-108 29 14     SPACE eurjchem-108 29 15 cm‐1 cm‐1 NOUN eurjchem-108 29 16 ): ): PUNCT eurjchem-108 29 17     SPACE eurjchem-108 29 18 3262 3262 NUM eurjchem-108 29 19 , , PUNCT eurjchem-108 29 20     SPACE eurjchem-108 29 21 2960 2960 NUM eurjchem-108 29 22 , , PUNCT eurjchem-108 29 23     SPACE eurjchem-108 29 24 1702 1702 NUM eurjchem-108 29 25 , , PUNCT eurjchem-108 29 26     SPACE eurjchem-108 29 27 1660 1660 NUM eurjchem-108 29 28 , , PUNCT eurjchem-108 29 29     SPACE eurjchem-108 29 30 1455 1455 NUM eurjchem-108 29 31 , , PUNCT eurjchem-108 29 32     SPACE eurjchem-108 29 33 1376 1376 NUM eurjchem-108 29 34 . . PUNCT eurjchem-108 29 35     SPACE eurjchem-108 30 1 1h‐nmr 1h‐nmr NUM eurjchem-108 30 2     SPACE eurjchem-108 30 3 ( ( PUNCT eurjchem-108 30 4 dmso‐d6 dmso‐d6 PROPN eurjchem-108 30 5 , , PUNCT eurjchem-108 30 6     SPACE eurjchem-108 30 7 δ δ PROPN eurjchem-108 30 8 , , PUNCT eurjchem-108 30 9     SPACE eurjchem-108 30 10 ppm ppm ADJ eurjchem-108 30 11 ): ): PUNCT eurjchem-108 30 12     SPACE eurjchem-108 30 13 0.89 0.89 NUM eurjchem-108 30 14     SPACE eurjchem-108 30 15 ( ( PUNCT eurjchem-108 30 16 s s PROPN eurjchem-108 30 17 , , PUNCT eurjchem-108 30 18     SPACE eurjchem-108 30 19 3h 3h NUM eurjchem-108 30 20 , , PUNCT eurjchem-108 30 21     SPACE eurjchem-108 30 22 ch3 ch3 PROPN eurjchem-108 30 23 ) ) PUNCT eurjchem-108 30 24 , , PUNCT eurjchem-108 30 25     SPACE eurjchem-108 30 26 1.02 1.02 NUM eurjchem-108 30 27     SPACE eurjchem-108 30 28 ( ( PUNCT eurjchem-108 30 29 s s PROPN eurjchem-108 30 30 , , PUNCT eurjchem-108 30 31     SPACE eurjchem-108 30 32 3h 3h NUM eurjchem-108 30 33 , , PUNCT eurjchem-108 30 34     SPACE eurjchem-108 30 35 ch3 ch3 PROPN eurjchem-108 30 36 ) ) PUNCT eurjchem-108 30 37 , , PUNCT eurjchem-108 30 38     SPACE eurjchem-108 30 39 2.00‐2.44 2.00‐2.44 NUM eurjchem-108 30 40     SPACE eurjchem-108 30 41 ( ( PUNCT eurjchem-108 30 42 m m PROPN eurjchem-108 30 43 , , PUNCT eurjchem-108 30 44     SPACE eurjchem-108 30 45 4h 4h NOUN eurjchem-108 30 46 , , PUNCT eurjchem-108 30 47     SPACE eurjchem-108 30 48 ch2‐8 ch2‐8 PROPN eurjchem-108 30 49 , , PUNCT eurjchem-108 30 50     SPACE eurjchem-108 30 51 ch2‐6 ch2‐6 NOUN eurjchem-108 30 52 ) ) PUNCT eurjchem-108 30 53 , , PUNCT eurjchem-108 30 54     SPACE eurjchem-108 30 55 5.14 5.14 NUM eurjchem-108 30 56     SPACE eurjchem-108 30 57 ( ( PUNCT eurjchem-108 30 58 d d PROPN eurjchem-108 30 59 , , PUNCT eurjchem-108 30 60     SPACE eurjchem-108 30 61 j=2.74 j=2.74 NOUN eurjchem-108 30 62     SPACE eurjchem-108 30 63 hz hz VERB eurjchem-108 30 64 , , PUNCT eurjchem-108 30 65     SPACE eurjchem-108 30 66 1h 1h NUM eurjchem-108 30 67 , , PUNCT eurjchem-108 30 68     SPACE eurjchem-108 30 69 h‐4 h‐4 NOUN eurjchem-108 30 70 ) ) PUNCT eurjchem-108 30 71 , , PUNCT eurjchem-108 30 72     SPACE eurjchem-108 30 73 7.19‐7.33 7.19‐7.33 NOUN eurjchem-108 30 74     SPACE eurjchem-108 30 75 ( ( PUNCT eurjchem-108 30 76 m m PROPN eurjchem-108 30 77 , , PUNCT eurjchem-108 30 78     SPACE eurjchem-108 30 79 5h 5h NUM eurjchem-108 30 80 , , PUNCT eurjchem-108 30 81     SPACE eurjchem-108 30 82 ar‐h ar‐h NOUN eurjchem-108 30 83 ) ) PUNCT eurjchem-108 30 84 , , PUNCT eurjchem-108 30 85     SPACE eurjchem-108 30 86 7.78 7.78 NUM eurjchem-108 30 87     SPACE eurjchem-108 30 88 ( ( PUNCT eurjchem-108 30 89 s s PROPN eurjchem-108 30 90 , , PUNCT eurjchem-108 30 91     SPACE eurjchem-108 30 92 1h 1h NUM eurjchem-108 30 93 , , PUNCT eurjchem-108 30 94     SPACE eurjchem-108 30 95 n3‐ n3‐ VERB eurjchem-108 30 96 h h NOUN eurjchem-108 30 97 ) ) PUNCT eurjchem-108 30 98 , , PUNCT eurjchem-108 30 99     SPACE eurjchem-108 30 100 9.48 9.48 NUM eurjchem-108 30 101     SPACE eurjchem-108 30 102 ( ( PUNCT eurjchem-108 30 103 s s PROPN eurjchem-108 30 104 , , PUNCT eurjchem-108 30 105     SPACE eurjchem-108 30 106 1h 1h NUM eurjchem-108 30 107 , , PUNCT eurjchem-108 30 108     SPACE eurjchem-108 30 109 n1‐h n1‐h PROPN eurjchem-108 30 110 ) ) PUNCT eurjchem-108 30 111 . . PUNCT eurjchem-108 30 112     SPACE eurjchem-108 31 1 anal anal ADJ eurjchem-108 31 2 . . PUNCT eurjchem-108 31 3     SPACE eurjchem-108 31 4 calcd calcd NOUN eurjchem-108 31 5 . . PUNCT eurjchem-108 31 6     SPACE eurjchem-108 31 7 for for ADP eurjchem-108 31 8     SPACE eurjchem-108 31 9 c16h18n2o2 c16h18n2o2 NOUN eurjchem-108 31 10 : : PUNCT eurjchem-108 31 11     SPACE eurjchem-108 31 12 c c X eurjchem-108 31 13 , , PUNCT eurjchem-108 31 14     SPACE eurjchem-108 31 15 71.09 71.09 NUM eurjchem-108 31 16 ; ; PUNCT eurjchem-108 31 17     SPACE eurjchem-108 31 18 h h NOUN eurjchem-108 31 19 , , PUNCT eurjchem-108 31 20     SPACE eurjchem-108 31 21 6.71 6.71 NUM eurjchem-108 31 22 ; ; PUNCT eurjchem-108 31 23     SPACE eurjchem-108 31 24 n n CCONJ eurjchem-108 31 25 , , PUNCT eurjchem-108 31 26     SPACE eurjchem-108 31 27 10.36 10.36 NUM eurjchem-108 31 28 % % NOUN eurjchem-108 31 29 . . PUNCT eurjchem-108 31 30     SPACE eurjchem-108 32 1 found find VERB eurjchem-108 32 2 : : PUNCT eurjchem-108 32 3     SPACE eurjchem-108 32 4 c c X eurjchem-108 32 5 , , PUNCT eurjchem-108 32 6     SPACE eurjchem-108 32 7 71.14 71.14 NUM eurjchem-108 32 8 ; ; PUNCT eurjchem-108 32 9     SPACE eurjchem-108 32 10 h h NOUN eurjchem-108 32 11 , , PUNCT eurjchem-108 32 12     SPACE eurjchem-108 32 13 6.62 6.62 NUM eurjchem-108 32 14 ; ; PUNCT eurjchem-108 32 15     SPACE eurjchem-108 32 16 n n CCONJ eurjchem-108 32 17     SPACE eurjchem-108 32 18 10.24 10.24 NUM eurjchem-108 32 19 % % NOUN eurjchem-108 32 20 . . PUNCT eurjchem-108 32 21     SPACE eurjchem-108 33 1 4­(3,4­dimethoxy)­7,7­dimethyl­1,2,3,4,5,6,7,8­octahydroqui 4­(3,4­dimethoxy)­7,7­dimethyl­1,2,3,4,5,6,7,8­octahydroqui NOUN eurjchem-108 33 2     SPACE eurjchem-108 33 3 nazoline­2,5­dione nazoline­2,5­dione NOUN eurjchem-108 33 4     SPACE eurjchem-108 33 5 ( ( PUNCT eurjchem-108 33 6 4c 4c NOUN eurjchem-108 33 7 ): ): PUNCT eurjchem-108 33 8     SPACE eurjchem-108 33 9 ir ir VERB eurjchem-108 33 10     SPACE eurjchem-108 33 11 ( ( PUNCT eurjchem-108 33 12 kbr kbr PROPN eurjchem-108 33 13 , , PUNCT eurjchem-108 33 14     SPACE eurjchem-108 33 15 cm‐1 cm‐1 PROPN eurjchem-108 33 16 ): ): PUNCT eurjchem-108 33 17     SPACE eurjchem-108 33 18 3244 3244 NUM eurjchem-108 33 19 , , PUNCT eurjchem-108 33 20     SPACE eurjchem-108 33 21 2959 2959 NUM eurjchem-108 33 22 , , PUNCT eurjchem-108 33 23     SPACE eurjchem-108 33 24 1701 1701 NUM eurjchem-108 33 25 , , PUNCT eurjchem-108 33 26     SPACE eurjchem-108 33 27 1629 1629 NUM eurjchem-108 33 28 , , PUNCT eurjchem-108 33 29     SPACE eurjchem-108 33 30 1516 1516 NUM eurjchem-108 33 31 , , PUNCT eurjchem-108 33 32     SPACE eurjchem-108 33 33 1376‐1451 1376‐1451 NUM eurjchem-108 33 34 . . PUNCT eurjchem-108 33 35     SPACE eurjchem-108 34 1 1h‐nmr 1h‐nmr NUM eurjchem-108 34 2     SPACE eurjchem-108 34 3 ( ( PUNCT eurjchem-108 34 4 dmso‐d6 dmso‐d6 PROPN eurjchem-108 34 5 , , PUNCT eurjchem-108 34 6     SPACE eurjchem-108 34 7 δ δ PROPN eurjchem-108 34 8 , , PUNCT eurjchem-108 34 9     SPACE eurjchem-108 34 10 ppm ppm ADJ eurjchem-108 34 11 ): ): PUNCT eurjchem-108 34 12     SPACE eurjchem-108 34 13 0.93 0.93 NUM eurjchem-108 34 14     SPACE eurjchem-108 34 15 ( ( PUNCT eurjchem-108 34 16 s s PROPN eurjchem-108 34 17 , , PUNCT eurjchem-108 34 18     SPACE eurjchem-108 34 19 3h 3h NUM eurjchem-108 34 20 , , PUNCT eurjchem-108 34 21     SPACE eurjchem-108 34 22 ch3 ch3 PROPN eurjchem-108 34 23 ) ) PUNCT eurjchem-108 34 24 , , PUNCT eurjchem-108 34 25     SPACE eurjchem-108 34 26 1.02 1.02 NUM eurjchem-108 34 27     SPACE eurjchem-108 34 28 ( ( PUNCT eurjchem-108 34 29 s s PROPN eurjchem-108 34 30 , , PUNCT eurjchem-108 34 31     SPACE eurjchem-108 34 32 3h 3h NUM eurjchem-108 34 33 , , PUNCT eurjchem-108 34 34     SPACE eurjchem-108 34 35 ch3 ch3 PROPN eurjchem-108 34 36 ) ) PUNCT eurjchem-108 34 37 , , PUNCT eurjchem-108 34 38     SPACE eurjchem-108 34 39 2.01‐2.45 2.01‐2.45 VERB eurjchem-108 34 40     SPACE eurjchem-108 34 41 ( ( PUNCT eurjchem-108 34 42 m m PROPN eurjchem-108 34 43 , , PUNCT eurjchem-108 34 44     SPACE eurjchem-108 34 45 4h 4h NOUN eurjchem-108 34 46 , , PUNCT eurjchem-108 34 47     SPACE eurjchem-108 34 48 ch2‐8 ch2‐8 PROPN eurjchem-108 34 49 , , PUNCT eurjchem-108 34 50     SPACE eurjchem-108 34 51 ch2‐6 ch2‐6 PROPN eurjchem-108 34 52 ) ) PUNCT eurjchem-108 34 53 , , PUNCT eurjchem-108 34 54     SPACE eurjchem-108 34 55 3.69 3.69 NUM eurjchem-108 34 56     SPACE eurjchem-108 34 57 ( ( PUNCT eurjchem-108 34 58 s s PROPN eurjchem-108 34 59 , , PUNCT eurjchem-108 34 60     SPACE eurjchem-108 34 61 3h 3h NUM eurjchem-108 34 62 , , PUNCT eurjchem-108 34 63     SPACE eurjchem-108 34 64 och3 och3 ADJ eurjchem-108 34 65 ) ) PUNCT eurjchem-108 34 66 , , PUNCT eurjchem-108 34 67     SPACE eurjchem-108 34 68 3.71 3.71 NUM eurjchem-108 34 69     SPACE eurjchem-108 34 70 ( ( PUNCT eurjchem-108 34 71 s s PROPN eurjchem-108 34 72 , , PUNCT eurjchem-108 34 73     SPACE eurjchem-108 34 74 3h 3h NUM eurjchem-108 34 75 , , PUNCT eurjchem-108 34 76     SPACE eurjchem-108 34 77 och3 och3 ADJ eurjchem-108 34 78 ) ) PUNCT eurjchem-108 34 79 , , PUNCT eurjchem-108 34 80     SPACE eurjchem-108 34 81 5.09 5.09 NUM eurjchem-108 34 82     SPACE eurjchem-108 34 83 ( ( PUNCT eurjchem-108 34 84 d d NOUN eurjchem-108 34 85 , , PUNCT eurjchem-108 34 86     SPACE eurjchem-108 34 87 j=2.61 j=2.61 NOUN eurjchem-108 34 88     SPACE eurjchem-108 34 89 hz hz NOUN eurjchem-108 34 90 , , PUNCT eurjchem-108 34 91     SPACE eurjchem-108 34 92 1h 1h NUM eurjchem-108 34 93 , , PUNCT eurjchem-108 34 94     SPACE eurjchem-108 34 95 h‐4 h‐4 NOUN eurjchem-108 34 96 ) ) PUNCT eurjchem-108 34 97 , , PUNCT eurjchem-108 34 98     SPACE eurjchem-108 34 99 6.70‐6.89 6.70‐6.89 NOUN eurjchem-108 34 100     SPACE eurjchem-108 34 101 ( ( PUNCT eurjchem-108 34 102 m m PROPN eurjchem-108 34 103 , , PUNCT eurjchem-108 34 104     SPACE eurjchem-108 34 105 3h 3h NUM eurjchem-108 34 106 , , PUNCT eurjchem-108 34 107     SPACE eurjchem-108 34 108 ar‐h ar‐h NOUN eurjchem-108 34 109 ) ) PUNCT eurjchem-108 34 110 , , PUNCT eurjchem-108 34 111     SPACE eurjchem-108 34 112 7.72 7.72 NUM eurjchem-108 34 113     SPACE eurjchem-108 34 114 ( ( PUNCT eurjchem-108 34 115 s s PROPN eurjchem-108 34 116 , , PUNCT eurjchem-108 34 117       SPACE eurjchem-108 34 118 1h 1h NUM eurjchem-108 34 119 , , PUNCT eurjchem-108 34 120       SPACE eurjchem-108 34 121 n3‐h n3‐h PROPN eurjchem-108 34 122 ) ) PUNCT eurjchem-108 34 123 , , PUNCT eurjchem-108 34 124     SPACE eurjchem-108 34 125 9.44 9.44 NUM eurjchem-108 34 126     SPACE eurjchem-108 34 127 ( ( PUNCT eurjchem-108 34 128 s s PROPN eurjchem-108 34 129 , , PUNCT eurjchem-108 34 130       SPACE eurjchem-108 34 131 1h 1h NUM eurjchem-108 34 132 , , PUNCT eurjchem-108 34 133       SPACE eurjchem-108 34 134 n1‐h n1‐h PROPN eurjchem-108 34 135 ) ) PUNCT eurjchem-108 34 136 . . PUNCT eurjchem-108 34 137     SPACE eurjchem-108 35 1 anal anal ADJ eurjchem-108 35 2 . . PUNCT eurjchem-108 35 3     SPACE eurjchem-108 35 4 calcd calcd NOUN eurjchem-108 35 5 . . PUNCT eurjchem-108 35 6     SPACE eurjchem-108 35 7 for for ADP eurjchem-108 35 8     SPACE eurjchem-108 35 9 c18h22n2o4 c18h22n2o4 NOUN eurjchem-108 35 10 : : PUNCT eurjchem-108 35 11     SPACE eurjchem-108 35 12 c c X eurjchem-108 35 13 , , PUNCT eurjchem-108 35 14     SPACE eurjchem-108 35 15 65.44 65.44 NUM eurjchem-108 35 16 ; ; PUNCT eurjchem-108 35 17     SPACE eurjchem-108 35 18 h h NOUN eurjchem-108 35 19 , , PUNCT eurjchem-108 35 20     SPACE eurjchem-108 35 21 6.71 6.71 NUM eurjchem-108 35 22 ; ; PUNCT eurjchem-108 35 23     SPACE eurjchem-108 35 24 n n CCONJ eurjchem-108 35 25 , , PUNCT eurjchem-108 35 26     SPACE eurjchem-108 35 27 8.48 8.48 NUM eurjchem-108 35 28 % % NOUN eurjchem-108 35 29 . . PUNCT eurjchem-108 35 30     SPACE eurjchem-108 35 31 found find VERB eurjchem-108 35 32 : : PUNCT eurjchem-108 35 33     SPACE eurjchem-108 35 34 c c X eurjchem-108 35 35 , , PUNCT eurjchem-108 35 36     SPACE eurjchem-108 35 37 65.32 65.32 NUM eurjchem-108 35 38 ; ; PUNCT eurjchem-108 35 39     SPACE eurjchem-108 35 40 h h NOUN eurjchem-108 35 41 , , PUNCT eurjchem-108 35 42     SPACE eurjchem-108 35 43 6.62 6.62 NUM eurjchem-108 35 44 ; ; PUNCT eurjchem-108 35 45     SPACE eurjchem-108 35 46 n n CCONJ eurjchem-108 35 47 , , PUNCT eurjchem-108 35 48     SPACE eurjchem-108 35 49 8.54 8.54 NUM eurjchem-108 35 50 % % NOUN eurjchem-108 35 51 . . PUNCT eurjchem-108 35 52     SPACE eurjchem-108 36 1 4‐(4‐fluorophenyl)‐7,7‐dimethyl‐1,2,3,4,5,6,7,8‐octahydro 4‐(4‐fluorophenyl)‐7,7‐dimethyl‐1,2,3,4,5,6,7,8‐octahydro NOUN eurjchem-108 36 2     SPACE eurjchem-108 36 3 quinazoline‐2,5‐dione quinazoline‐2,5‐dione NOUN eurjchem-108 36 4     SPACE eurjchem-108 36 5 ( ( PUNCT eurjchem-108 36 6 4d 4d NUM eurjchem-108 36 7 ): ): PUNCT eurjchem-108 36 8     SPACE eurjchem-108 36 9 ir ir VERB eurjchem-108 36 10     SPACE eurjchem-108 36 11 ( ( PUNCT eurjchem-108 36 12 kbr kbr PROPN eurjchem-108 36 13 , , PUNCT eurjchem-108 36 14     SPACE eurjchem-108 36 15 cm‐1 cm‐1 NOUN eurjchem-108 36 16 ): ): PUNCT eurjchem-108 36 17     SPACE eurjchem-108 36 18 3239 3239 NUM eurjchem-108 36 19 , , PUNCT eurjchem-108 36 20     SPACE eurjchem-108 36 21 2952 2952 NUM eurjchem-108 36 22 , , PUNCT eurjchem-108 36 23     SPACE eurjchem-108 36 24 1697 1697 NUM eurjchem-108 36 25 , , PUNCT eurjchem-108 36 26     SPACE eurjchem-108 36 27 1631 1631 NUM eurjchem-108 36 28 , , PUNCT eurjchem-108 36 29     SPACE eurjchem-108 36 30 1509 1509 NUM eurjchem-108 36 31 , , PUNCT eurjchem-108 36 32     SPACE eurjchem-108 36 33 1377‐1447 1377‐1447 NUM eurjchem-108 36 34 . . PUNCT eurjchem-108 36 35     SPACE eurjchem-108 36 36 1h‐nmr 1h‐nmr NUM eurjchem-108 36 37     SPACE eurjchem-108 36 38 ( ( PUNCT eurjchem-108 36 39 dmso‐d6 dmso‐d6 PROPN eurjchem-108 36 40 , , PUNCT eurjchem-108 36 41     SPACE eurjchem-108 36 42 δ δ PROPN eurjchem-108 36 43 , , PUNCT eurjchem-108 36 44     SPACE eurjchem-108 36 45 ppm ppm NOUN eurjchem-108 36 46 ): ): PUNCT eurjchem-108 36 47     SPACE eurjchem-108 36 48 0.89 0.89 NUM eurjchem-108 36 49     SPACE eurjchem-108 36 50 ( ( PUNCT eurjchem-108 36 51 s s PROPN eurjchem-108 36 52 , , PUNCT eurjchem-108 36 53     SPACE eurjchem-108 36 54 3h 3h NUM eurjchem-108 36 55 , , PUNCT eurjchem-108 36 56     SPACE eurjchem-108 36 57 ch3 ch3 PROPN eurjchem-108 36 58 ) ) PUNCT eurjchem-108 36 59 , , PUNCT eurjchem-108 36 60 1.01 1.01 NUM eurjchem-108 36 61     SPACE eurjchem-108 36 62 ( ( PUNCT eurjchem-108 36 63 s s PROPN eurjchem-108 36 64 , , PUNCT eurjchem-108 36 65     SPACE eurjchem-108 36 66 3h 3h NUM eurjchem-108 36 67 , , PUNCT eurjchem-108 36 68     SPACE eurjchem-108 36 69 ch3 ch3 PROPN eurjchem-108 36 70 ) ) PUNCT eurjchem-108 36 71 , , PUNCT eurjchem-108 36 72     SPACE eurjchem-108 36 73 2.00‐2.44 2.00‐2.44 NUM eurjchem-108 36 74     SPACE eurjchem-108 36 75 ( ( PUNCT eurjchem-108 36 76 m m PROPN eurjchem-108 36 77 , , PUNCT eurjchem-108 36 78     SPACE eurjchem-108 36 79 4h 4h NOUN eurjchem-108 36 80 , , PUNCT eurjchem-108 36 81     SPACE eurjchem-108 36 82 ch2‐8 ch2‐8 PROPN eurjchem-108 36 83 , , PUNCT eurjchem-108 36 84     SPACE eurjchem-108 36 85 ch2‐6 ch2‐6 NOUN eurjchem-108 36 86 ) ) PUNCT eurjchem-108 36 87 , , PUNCT eurjchem-108 36 88     SPACE eurjchem-108 36 89 5.16 5.16 NUM eurjchem-108 36 90     SPACE eurjchem-108 36 91 ( ( PUNCT eurjchem-108 36 92 s s PROPN eurjchem-108 36 93 , , PUNCT eurjchem-108 36 94     SPACE eurjchem-108 36 95 1h 1h NUM eurjchem-108 36 96 , , PUNCT eurjchem-108 36 97     SPACE eurjchem-108 36 98 h‐4 h‐4 NOUN eurjchem-108 36 99 ) ) PUNCT eurjchem-108 36 100 , , PUNCT eurjchem-108 36 101     SPACE eurjchem-108 36 102 7.10‐7.28 7.10‐7.28 NOUN eurjchem-108 36 103     SPACE eurjchem-108 36 104 ( ( PUNCT eurjchem-108 36 105 m m PROPN eurjchem-108 36 106 , , PUNCT eurjchem-108 36 107     SPACE eurjchem-108 36 108 4h 4h NOUN eurjchem-108 36 109 , , PUNCT eurjchem-108 36 110     SPACE eurjchem-108 36 111 h h NOUN eurjchem-108 36 112     SPACE eurjchem-108 36 113 aromatic aromatic NOUN eurjchem-108 36 114 ) ) PUNCT eurjchem-108 36 115 , , PUNCT eurjchem-108 36 116     SPACE eurjchem-108 36 117 7.75 7.75 NUM eurjchem-108 36 118     SPACE eurjchem-108 36 119 ( ( PUNCT eurjchem-108 36 120 s s PROPN eurjchem-108 36 121 , , PUNCT eurjchem-108 36 122       SPACE eurjchem-108 36 123 1h 1h NUM eurjchem-108 36 124 , , PUNCT eurjchem-108 36 125       SPACE eurjchem-108 36 126 n3‐ n3‐ VERB eurjchem-108 36 127 h h NOUN eurjchem-108 36 128 ) ) PUNCT eurjchem-108 36 129 , , PUNCT eurjchem-108 36 130     SPACE eurjchem-108 36 131 9.47 9.47 NUM eurjchem-108 36 132     SPACE eurjchem-108 36 133 ( ( PUNCT eurjchem-108 36 134 s s PROPN eurjchem-108 36 135 , , PUNCT eurjchem-108 36 136       SPACE eurjchem-108 36 137 1h 1h NUM eurjchem-108 36 138 , , PUNCT eurjchem-108 36 139       SPACE eurjchem-108 36 140 n1‐h n1‐h PROPN eurjchem-108 36 141 ) ) PUNCT eurjchem-108 36 142 . . PUNCT eurjchem-108 36 143     SPACE eurjchem-108 37 1 anal anal ADJ eurjchem-108 37 2 . . PUNCT eurjchem-108 37 3     SPACE eurjchem-108 37 4 calcd calcd NOUN eurjchem-108 37 5 . . PUNCT eurjchem-108 37 6     SPACE eurjchem-108 37 7 for for ADP eurjchem-108 37 8     SPACE eurjchem-108 37 9 c16h17fn2o2 c16h17fn2o2 NOUN eurjchem-108 37 10 : : PUNCT eurjchem-108 37 11     SPACE eurjchem-108 37 12 c c X eurjchem-108 37 13 , , PUNCT eurjchem-108 37 14     SPACE eurjchem-108 37 15 66.65 66.65 NUM eurjchem-108 37 16 ; ; PUNCT eurjchem-108 37 17     SPACE eurjchem-108 37 18 h h NOUN eurjchem-108 37 19 , , PUNCT eurjchem-108 37 20     SPACE eurjchem-108 37 21 5.94 5.94 NUM eurjchem-108 37 22 ; ; PUNCT eurjchem-108 37 23     SPACE eurjchem-108 37 24 n n CCONJ eurjchem-108 37 25 , , PUNCT eurjchem-108 37 26     SPACE eurjchem-108 37 27 9.72 9.72 NUM eurjchem-108 37 28 % % NOUN eurjchem-108 37 29 . . PUNCT eurjchem-108 37 30     SPACE eurjchem-108 37 31 found find VERB eurjchem-108 37 32 : : PUNCT eurjchem-108 37 33     SPACE eurjchem-108 37 34 c c X eurjchem-108 37 35 , , PUNCT eurjchem-108 37 36     SPACE eurjchem-108 37 37 66.78 66.78 NUM eurjchem-108 37 38 ; ; PUNCT eurjchem-108 37 39     SPACE eurjchem-108 37 40 h h NOUN eurjchem-108 37 41 , , PUNCT eurjchem-108 37 42     SPACE eurjchem-108 37 43 5.91 5.91 NUM eurjchem-108 37 44 ; ; PUNCT eurjchem-108 37 45     SPACE eurjchem-108 37 46 n n CCONJ eurjchem-108 37 47 , , PUNCT eurjchem-108 37 48     SPACE eurjchem-108 37 49 9.61 9.61 NUM eurjchem-108 37 50 % % NOUN eurjchem-108 37 51 . . PUNCT eurjchem-108 37 52     SPACE eurjchem-108 38 1 4­(4­nitrophenyl)­7,7­dimethyl­1,2,3,4,5,6,7,8­octahydroquin 4­(4­nitrophenyl)­7,7­dimethyl­1,2,3,4,5,6,7,8­octahydroquin NOUN eurjchem-108 38 2     SPACE eurjchem-108 39 1 azoline­2,5­dione azoline­2,5­dione NOUN eurjchem-108 39 2     SPACE eurjchem-108 39 3 ( ( PUNCT eurjchem-108 39 4 4i 4i NUM eurjchem-108 39 5 ): ): PUNCT eurjchem-108 39 6     SPACE eurjchem-108 39 7 ir ir VERB eurjchem-108 39 8     SPACE eurjchem-108 39 9 ( ( PUNCT eurjchem-108 39 10 kbr kbr PROPN eurjchem-108 39 11 , , PUNCT eurjchem-108 39 12     SPACE eurjchem-108 39 13 cm‐1 cm‐1 NOUN eurjchem-108 39 14 ): ): PUNCT eurjchem-108 39 15     SPACE eurjchem-108 39 16 3248 3248 NUM eurjchem-108 39 17 , , PUNCT eurjchem-108 39 18     SPACE eurjchem-108 39 19 2962 2962 NUM eurjchem-108 39 20 , , PUNCT eurjchem-108 39 21     SPACE eurjchem-108 39 22 1704 1704 NUM eurjchem-108 39 23 , , PUNCT eurjchem-108 39 24     SPACE eurjchem-108 39 25 1625 1625 NUM eurjchem-108 39 26 , , PUNCT eurjchem-108 39 27     SPACE eurjchem-108 39 28 1523 1523 NUM eurjchem-108 39 29 , , PUNCT eurjchem-108 39 30     SPACE eurjchem-108 39 31 1349‐1447 1349‐1447 NUM eurjchem-108 39 32 . . PUNCT eurjchem-108 39 33     SPACE eurjchem-108 40 1 1h‐nmr 1h‐nmr NUM eurjchem-108 40 2     SPACE eurjchem-108 40 3 ( ( PUNCT eurjchem-108 40 4 dmso‐d6 dmso‐d6 PROPN eurjchem-108 40 5 , , PUNCT eurjchem-108 40 6     SPACE eurjchem-108 40 7 δ δ PROPN eurjchem-108 40 8 , , PUNCT eurjchem-108 40 9     SPACE eurjchem-108 40 10 ppm ppm ADJ eurjchem-108 40 11 ): ): PUNCT eurjchem-108 40 12     SPACE eurjchem-108 40 13 0.87 0.87 NUM eurjchem-108 40 14     SPACE eurjchem-108 40 15 ( ( PUNCT eurjchem-108 40 16 s s PROPN eurjchem-108 40 17 , , PUNCT eurjchem-108 40 18     SPACE eurjchem-108 40 19 3h 3h NUM eurjchem-108 40 20 , , PUNCT eurjchem-108 40 21     SPACE eurjchem-108 40 22 ch3 ch3 PROPN eurjchem-108 40 23 ) ) PUNCT eurjchem-108 40 24 , , PUNCT eurjchem-108 40 25 1.02 1.02 NUM eurjchem-108 40 26     SPACE eurjchem-108 40 27 ( ( PUNCT eurjchem-108 40 28 s s PROPN eurjchem-108 40 29 , , PUNCT eurjchem-108 40 30     SPACE eurjchem-108 40 31 3h 3h NUM eurjchem-108 40 32 , , PUNCT eurjchem-108 40 33     SPACE eurjchem-108 40 34 ch3 ch3 PROPN eurjchem-108 40 35 ) ) PUNCT eurjchem-108 40 36 , , PUNCT eurjchem-108 40 37     SPACE eurjchem-108 40 38 2.00‐2.46 2.00‐2.46 NUM eurjchem-108 40 39     SPACE eurjchem-108 40 40 ( ( PUNCT eurjchem-108 40 41 m m PROPN eurjchem-108 40 42 , , PUNCT eurjchem-108 40 43     SPACE eurjchem-108 40 44 4h 4h NOUN eurjchem-108 40 45 , , PUNCT eurjchem-108 40 46     SPACE eurjchem-108 40 47 ch2‐8 ch2‐8 PROPN eurjchem-108 40 48 , , PUNCT eurjchem-108 40 49     SPACE eurjchem-108 40 50 ch2‐6 ch2‐6 PROPN eurjchem-108 40 51 ) ) PUNCT eurjchem-108 40 52 , , PUNCT eurjchem-108 40 53     SPACE eurjchem-108 40 54 5.30 5.30 NUM eurjchem-108 40 55     SPACE eurjchem-108 40 56 ( ( PUNCT eurjchem-108 40 57 d d NOUN eurjchem-108 40 58 , , PUNCT eurjchem-108 40 59     SPACE eurjchem-108 40 60 j=2.75 j=2.75 NOUN eurjchem-108 40 61     SPACE eurjchem-108 40 62 hz hz VERB eurjchem-108 40 63 , , PUNCT eurjchem-108 40 64     SPACE eurjchem-108 40 65 1h 1h NUM eurjchem-108 40 66 , , PUNCT eurjchem-108 40 67     SPACE eurjchem-108 40 68 h‐4 h‐4 NOUN eurjchem-108 40 69 ) ) PUNCT eurjchem-108 40 70 , , PUNCT eurjchem-108 40 71     SPACE eurjchem-108 40 72 7.51 7.51 NUM eurjchem-108 40 73     SPACE eurjchem-108 40 74 ( ( PUNCT eurjchem-108 40 75 d d PROPN eurjchem-108 40 76 , , PUNCT eurjchem-108 40 77     SPACE eurjchem-108 40 78 j=8.76 j=8.76 NOUN eurjchem-108 40 79     SPACE eurjchem-108 40 80 hz hz VERB eurjchem-108 40 81 , , PUNCT eurjchem-108 40 82     SPACE eurjchem-108 40 83 2h 2h NUM eurjchem-108 40 84 , , PUNCT eurjchem-108 40 85     SPACE eurjchem-108 40 86 ar‐h ar‐h NOUN eurjchem-108 40 87 ) ) PUNCT eurjchem-108 40 88 , , PUNCT eurjchem-108 40 89     SPACE eurjchem-108 40 90 7.89 7.89 NUM eurjchem-108 40 91     SPACE eurjchem-108 40 92 ( ( PUNCT eurjchem-108 40 93 s s PROPN eurjchem-108 40 94 , , PUNCT eurjchem-108 40 95       SPACE eurjchem-108 40 96 1h 1h NUM eurjchem-108 40 97 , , PUNCT eurjchem-108 40 98         SPACE eurjchem-108 40 99 n3‐h n3‐h PROPN eurjchem-108 40 100 ) ) PUNCT eurjchem-108 40 101 , , PUNCT eurjchem-108 40 102     SPACE eurjchem-108 40 103 8.20 8.20 NUM eurjchem-108 40 104     SPACE eurjchem-108 40 105 ( ( PUNCT eurjchem-108 40 106 d d PROPN eurjchem-108 40 107 , , PUNCT eurjchem-108 40 108     SPACE eurjchem-108 40 109 j=8.78 j=8.78 PROPN eurjchem-108 40 110     SPACE eurjchem-108 40 111 hz hz VERB eurjchem-108 40 112 , , PUNCT eurjchem-108 40 113 2h 2h NUM eurjchem-108 40 114 , , PUNCT eurjchem-108 40 115     SPACE eurjchem-108 40 116 ar‐h ar‐h NOUN eurjchem-108 40 117 ) ) PUNCT eurjchem-108 40 118 , , PUNCT eurjchem-108 40 119     SPACE eurjchem-108 40 120 9.60 9.60 NUM eurjchem-108 40 121     SPACE eurjchem-108 40 122 ( ( PUNCT eurjchem-108 40 123 s s PROPN eurjchem-108 40 124 , , PUNCT eurjchem-108 40 125         SPACE eurjchem-108 40 126 1h 1h NUM eurjchem-108 40 127 , , PUNCT eurjchem-108 40 128         SPACE eurjchem-108 40 129 n1‐h n1‐h PROPN eurjchem-108 40 130 ) ) PUNCT eurjchem-108 40 131 . . PUNCT eurjchem-108 40 132     SPACE eurjchem-108 41 1 anal anal ADJ eurjchem-108 41 2 . . PUNCT eurjchem-108 41 3     SPACE eurjchem-108 41 4 calcd calcd NOUN eurjchem-108 41 5 . . PUNCT eurjchem-108 41 6     SPACE eurjchem-108 41 7 for for ADP eurjchem-108 41 8     SPACE eurjchem-108 41 9 c16h17n3o4 c16h17n3o4 PROPN eurjchem-108 41 10 : : PUNCT eurjchem-108 41 11     SPACE eurjchem-108 41 12 c c X eurjchem-108 41 13 , , PUNCT eurjchem-108 41 14     SPACE eurjchem-108 41 15 60.95 60.95 NUM eurjchem-108 41 16 ; ; PUNCT eurjchem-108 41 17     SPACE eurjchem-108 41 18 h h NOUN eurjchem-108 41 19 , , PUNCT eurjchem-108 41 20     SPACE eurjchem-108 41 21 5.43 5.43 NUM eurjchem-108 41 22 ; ; PUNCT eurjchem-108 41 23     SPACE eurjchem-108 41 24 n n CCONJ eurjchem-108 41 25 , , PUNCT eurjchem-108 41 26     SPACE eurjchem-108 41 27 13.33 13.33 NUM eurjchem-108 41 28 % % NOUN eurjchem-108 41 29 . . PUNCT eurjchem-108 41 30     SPACE eurjchem-108 41 31 found find VERB eurjchem-108 41 32 : : PUNCT eurjchem-108 41 33     SPACE eurjchem-108 41 34 c c X eurjchem-108 41 35 , , PUNCT eurjchem-108 41 36     SPACE eurjchem-108 41 37 61.21 61.21 NUM eurjchem-108 41 38 ; ; PUNCT eurjchem-108 41 39     SPACE eurjchem-108 41 40 h h NOUN eurjchem-108 41 41 , , PUNCT eurjchem-108 41 42     SPACE eurjchem-108 41 43 5.51 5.51 NUM eurjchem-108 41 44 ; ; PUNCT eurjchem-108 41 45     SPACE eurjchem-108 41 46 n n CCONJ eurjchem-108 41 47 , , PUNCT eurjchem-108 41 48     SPACE eurjchem-108 41 49 13.19 13.19 NUM eurjchem-108 41 50 % % NOUN eurjchem-108 41 51 . . PUNCT eurjchem-108 41 52     SPACE eurjchem-108 42 1 4­(4­methylphenyl)­7,7­dimethyl­5­oxo­1,2,3,4,5,6,7,8­octa 4­(4­methylphenyl)­7,7­dimethyl­5­oxo­1,2,3,4,5,6,7,8­octa NUM eurjchem-108 42 2     SPACE eurjchem-108 42 3 hydroquinazoline­2­thione hydroquinazoline­2­thione NOUN eurjchem-108 42 4     SPACE eurjchem-108 42 5 ( ( PUNCT eurjchem-108 42 6 4k 4k NOUN eurjchem-108 42 7 ): ): PUNCT eurjchem-108 42 8     SPACE eurjchem-108 42 9 ir ir NOUN eurjchem-108 42 10     SPACE eurjchem-108 42 11 ( ( PUNCT eurjchem-108 42 12 kbr kbr PROPN eurjchem-108 42 13 , , PUNCT eurjchem-108 42 14     SPACE eurjchem-108 42 15 cm‐1 cm‐1 NOUN eurjchem-108 42 16 ): ): PUNCT eurjchem-108 42 17     SPACE eurjchem-108 42 18 3165 3165 NUM eurjchem-108 42 19 , , PUNCT eurjchem-108 42 20     SPACE eurjchem-108 42 21 2949 2949 NUM eurjchem-108 42 22 , , PUNCT eurjchem-108 42 23     SPACE eurjchem-108 42 24 1640 1640 NUM eurjchem-108 42 25 , , PUNCT eurjchem-108 42 26     SPACE eurjchem-108 42 27 1572 1572 NUM eurjchem-108 42 28 , , PUNCT eurjchem-108 42 29     SPACE eurjchem-108 42 30 1475 1475 NUM eurjchem-108 42 31 . . PUNCT eurjchem-108 42 32     SPACE eurjchem-108 43 1 1h‐nmr 1h‐nmr NUM eurjchem-108 43 2     SPACE eurjchem-108 43 3 ( ( PUNCT eurjchem-108 43 4 dmso‐d6 dmso‐d6 PROPN eurjchem-108 43 5 , , PUNCT eurjchem-108 43 6     SPACE eurjchem-108 43 7 δ δ PROPN eurjchem-108 43 8 , , PUNCT eurjchem-108 43 9     SPACE eurjchem-108 43 10 ppm ppm NOUN eurjchem-108 43 11 ): ): PUNCT eurjchem-108 43 12     SPACE eurjchem-108 43 13 0.88 0.88 NUM eurjchem-108 43 14     SPACE eurjchem-108 43 15 ( ( PUNCT eurjchem-108 43 16 s s PROPN eurjchem-108 43 17 , , PUNCT eurjchem-108 43 18     SPACE eurjchem-108 43 19 3h 3h NUM eurjchem-108 43 20 , , PUNCT eurjchem-108 43 21     SPACE eurjchem-108 43 22 ch3 ch3 PROPN eurjchem-108 43 23 ) ) PUNCT eurjchem-108 43 24 , , PUNCT eurjchem-108 43 25 1.02 1.02 NUM eurjchem-108 43 26     SPACE eurjchem-108 43 27 ( ( PUNCT eurjchem-108 43 28 s s PROPN eurjchem-108 43 29 , , PUNCT eurjchem-108 43 30     SPACE eurjchem-108 43 31 3h 3h NUM eurjchem-108 43 32 , , PUNCT eurjchem-108 43 33     SPACE eurjchem-108 43 34 ch3 ch3 PROPN eurjchem-108 43 35 ) ) PUNCT eurjchem-108 43 36 , , PUNCT eurjchem-108 43 37     SPACE eurjchem-108 43 38 2.02‐2.47 2.02‐2.47 NUM eurjchem-108 43 39     SPACE eurjchem-108 43 40 ( ( PUNCT eurjchem-108 43 41 m m PROPN eurjchem-108 43 42 , , PUNCT eurjchem-108 43 43     SPACE eurjchem-108 43 44 7h 7h NUM eurjchem-108 43 45 , , PUNCT eurjchem-108 43 46     SPACE eurjchem-108 43 47 ch2‐8 ch2‐8 PROPN eurjchem-108 43 48 , , PUNCT eurjchem-108 43 49     SPACE eurjchem-108 43 50 ch2‐6 ch2‐6 PROPN eurjchem-108 43 51 , , PUNCT eurjchem-108 43 52     SPACE eurjchem-108 43 53 ar‐ ar‐ PROPN eurjchem-108 43 54 ch3 ch3 PROPN eurjchem-108 43 55 ) ) PUNCT eurjchem-108 43 56 , , PUNCT eurjchem-108 43 57     SPACE eurjchem-108 43 58 5.13 5.13 NUM eurjchem-108 43 59     SPACE eurjchem-108 43 60 ( ( PUNCT eurjchem-108 43 61 s s PROPN eurjchem-108 43 62 , , PUNCT eurjchem-108 43 63     SPACE eurjchem-108 43 64 1h 1h NUM eurjchem-108 43 65 , , PUNCT eurjchem-108 43 66     SPACE eurjchem-108 43 67 h‐4 h‐4 NOUN eurjchem-108 43 68 ) ) PUNCT eurjchem-108 43 69 , , PUNCT eurjchem-108 43 70     SPACE eurjchem-108 43 71 7.07‐7.14 7.07‐7.14 NUM eurjchem-108 43 72     SPACE eurjchem-108 43 73 ( ( PUNCT eurjchem-108 43 74 m m PROPN eurjchem-108 43 75 , , PUNCT eurjchem-108 43 76     SPACE eurjchem-108 43 77 4h 4h NOUN eurjchem-108 43 78 , , PUNCT eurjchem-108 43 79     SPACE eurjchem-108 43 80 ar‐h ar‐h NOUN eurjchem-108 43 81 ) ) PUNCT eurjchem-108 43 82 , , PUNCT eurjchem-108 43 83     SPACE eurjchem-108 43 84 9.61 9.61 NUM eurjchem-108 43 85     SPACE eurjchem-108 43 86 ( ( PUNCT eurjchem-108 43 87 s s PROPN eurjchem-108 43 88 , , PUNCT eurjchem-108 43 89       SPACE eurjchem-108 43 90 1h 1h NUM eurjchem-108 43 91 , , PUNCT eurjchem-108 43 92       SPACE eurjchem-108 43 93 n3‐ n3‐ VERB eurjchem-108 43 94 h h NOUN eurjchem-108 43 95 ) ) PUNCT eurjchem-108 43 96 , , PUNCT eurjchem-108 43 97     SPACE eurjchem-108 43 98 10.51 10.51 NUM eurjchem-108 43 99     SPACE eurjchem-108 43 100 ( ( PUNCT eurjchem-108 43 101 s s PROPN eurjchem-108 43 102 , , PUNCT eurjchem-108 43 103       SPACE eurjchem-108 43 104 1h 1h NUM eurjchem-108 43 105 , , PUNCT eurjchem-108 43 106       SPACE eurjchem-108 43 107 n1‐h n1‐h PROPN eurjchem-108 43 108 ) ) PUNCT eurjchem-108 43 109 . . PUNCT eurjchem-108 43 110     SPACE eurjchem-108 44 1 anal anal ADJ eurjchem-108 44 2 . . PUNCT eurjchem-108 44 3     SPACE eurjchem-108 44 4 calcd calcd NOUN eurjchem-108 44 5 . . PUNCT eurjchem-108 44 6     SPACE eurjchem-108 44 7 for for ADP eurjchem-108 44 8     SPACE eurjchem-108 44 9 c17h20n2os c17h20n2o NOUN eurjchem-108 44 10 : : PUNCT eurjchem-108 44 11     SPACE eurjchem-108 44 12 c c X eurjchem-108 44 13 , , PUNCT eurjchem-108 44 14     SPACE eurjchem-108 44 15 67.97 67.97 NUM eurjchem-108 44 16 ; ; PUNCT eurjchem-108 44 17     SPACE eurjchem-108 44 18 h h NOUN eurjchem-108 44 19 , , PUNCT eurjchem-108 44 20     SPACE eurjchem-108 44 21 6.71 6.71 NUM eurjchem-108 44 22 ; ; PUNCT eurjchem-108 44 23     SPACE eurjchem-108 44 24 n n CCONJ eurjchem-108 44 25 , , PUNCT eurjchem-108 44 26     SPACE eurjchem-108 44 27 9.32 9.32 NUM eurjchem-108 44 28 ; ; PUNCT eurjchem-108 44 29     SPACE eurjchem-108 44 30 % % NOUN eurjchem-108 44 31 . . PUNCT eurjchem-108 44 32     SPACE eurjchem-108 44 33 found find VERB eurjchem-108 44 34 : : PUNCT eurjchem-108 44 35     SPACE eurjchem-108 44 36 c c X eurjchem-108 44 37 , , PUNCT eurjchem-108 44 38     SPACE eurjchem-108 44 39 68.15 68.15 NUM eurjchem-108 44 40 ; ; PUNCT eurjchem-108 44 41     SPACE eurjchem-108 44 42 h h NOUN eurjchem-108 44 43 , , PUNCT eurjchem-108 44 44     SPACE eurjchem-108 44 45 6.49 6.49 NUM eurjchem-108 44 46 ; ; PUNCT eurjchem-108 44 47     SPACE eurjchem-108 44 48 n n CCONJ eurjchem-108 44 49 , , PUNCT eurjchem-108 44 50     SPACE eurjchem-108 44 51 9.54 9.54 NUM eurjchem-108 44 52 % % NOUN eurjchem-108 44 53 . . PUNCT eurjchem-108 44 54     SPACE eurjchem-108 45 1 4­(3,4­dimethoxyphenyl)­7,7­dimethyl­5­oxo­1,2,3,4,5,6,7,8­ 4­(3,4­dimethoxyphenyl)­7,7­dimethyl­5­oxo­1,2,3,4,5,6,7,8­ NUM eurjchem-108 46 1 octahydroquinazoline­2­thione octahydroquinazoline­2­thione NOUN eurjchem-108 46 2     SPACE eurjchem-108 46 3 ( ( PUNCT eurjchem-108 46 4 4l 4l NOUN eurjchem-108 46 5 ): ): PUNCT eurjchem-108 46 6     SPACE eurjchem-108 46 7 ir ir VERB eurjchem-108 46 8     SPACE eurjchem-108 46 9 ( ( PUNCT eurjchem-108 46 10 kbr kbr PROPN eurjchem-108 46 11 , , PUNCT eurjchem-108 46 12     SPACE eurjchem-108 46 13 cm‐1 cm‐1 PROPN eurjchem-108 46 14 ): ): PUNCT eurjchem-108 46 15     SPACE eurjchem-108 46 16 3285 3285 NUM eurjchem-108 46 17 , , PUNCT eurjchem-108 46 18     SPACE eurjchem-108 46 19 2958 2958 NUM eurjchem-108 46 20 , , PUNCT eurjchem-108 46 21     SPACE eurjchem-108 46 22 1627 1627 NUM eurjchem-108 46 23 , , PUNCT eurjchem-108 46 24     SPACE eurjchem-108 46 25 1559 1559 NUM eurjchem-108 46 26 , , PUNCT eurjchem-108 46 27     SPACE eurjchem-108 46 28 1457 1457 NUM eurjchem-108 46 29 . . PUNCT eurjchem-108 46 30     SPACE eurjchem-108 47 1 1h‐nmr 1h‐nmr NUM eurjchem-108 47 2     SPACE eurjchem-108 47 3 ( ( PUNCT eurjchem-108 47 4 dmso‐d6 dmso‐d6 PROPN eurjchem-108 47 5 , , PUNCT eurjchem-108 47 6     SPACE eurjchem-108 47 7 δ δ PROPN eurjchem-108 47 8 , , PUNCT eurjchem-108 47 9     SPACE eurjchem-108 47 10 ppm ppm ADJ eurjchem-108 47 11 ): ): PUNCT eurjchem-108 47 12     SPACE eurjchem-108 47 13 0.93 0.93 NUM eurjchem-108 47 14     SPACE eurjchem-108 47 15 ( ( PUNCT eurjchem-108 47 16 s s PROPN eurjchem-108 47 17 , , PUNCT eurjchem-108 47 18     SPACE eurjchem-108 47 19 3h 3h NUM eurjchem-108 47 20 , , PUNCT eurjchem-108 47 21     SPACE eurjchem-108 47 22 ch3 ch3 PROPN eurjchem-108 47 23 ) ) PUNCT eurjchem-108 47 24 , , PUNCT eurjchem-108 47 25     SPACE eurjchem-108 47 26 1.03 1.03 NUM eurjchem-108 47 27     SPACE eurjchem-108 47 28 ( ( PUNCT eurjchem-108 47 29 s s PROPN eurjchem-108 47 30 , , PUNCT eurjchem-108 47 31     SPACE eurjchem-108 47 32 3h 3h NUM eurjchem-108 47 33 , , PUNCT eurjchem-108 47 34     SPACE eurjchem-108 47 35 ch3 ch3 PROPN eurjchem-108 47 36 ) ) PUNCT eurjchem-108 47 37 , , PUNCT eurjchem-108 47 38     SPACE eurjchem-108 47 39 2.05‐2.42 2.05‐2.42 NUM eurjchem-108 47 40     SPACE eurjchem-108 47 41 ( ( PUNCT eurjchem-108 47 42 m m PROPN eurjchem-108 47 43 , , PUNCT eurjchem-108 47 44     SPACE eurjchem-108 47 45 4h 4h NOUN eurjchem-108 47 46 , , PUNCT eurjchem-108 47 47     SPACE eurjchem-108 47 48 ch2‐8 ch2‐8 PROPN eurjchem-108 47 49 , , PUNCT eurjchem-108 47 50     SPACE eurjchem-108 47 51 ch2‐6 ch2‐6 PROPN eurjchem-108 47 52 ) ) PUNCT eurjchem-108 47 53 , , PUNCT eurjchem-108 47 54     SPACE eurjchem-108 47 55 3.70 3.70 NUM eurjchem-108 47 56     SPACE eurjchem-108 47 57 ( ( PUNCT eurjchem-108 47 58 s s PROPN eurjchem-108 47 59 , , PUNCT eurjchem-108 47 60     SPACE eurjchem-108 47 61 3h 3h NUM eurjchem-108 47 62 , , PUNCT eurjchem-108 47 63     SPACE eurjchem-108 47 64 och3 och3 ADJ eurjchem-108 47 65 ) ) PUNCT eurjchem-108 47 66 , , PUNCT eurjchem-108 47 67     SPACE eurjchem-108 47 68 3.71 3.71 NUM eurjchem-108 47 69     SPACE eurjchem-108 47 70 ( ( PUNCT eurjchem-108 47 71 s s PROPN eurjchem-108 47 72 , , PUNCT eurjchem-108 47 73     SPACE eurjchem-108 47 74 3h 3h NUM eurjchem-108 47 75 , , PUNCT eurjchem-108 47 76     SPACE eurjchem-108 47 77 och3 och3 ADJ eurjchem-108 47 78 ) ) PUNCT eurjchem-108 47 79 , , PUNCT eurjchem-108 47 80     SPACE eurjchem-108 47 81 5.11 5.11 NUM eurjchem-108 47 82     SPACE eurjchem-108 47 83 ( ( PUNCT eurjchem-108 47 84 s s PROPN eurjchem-108 47 85 , , PUNCT eurjchem-108 47 86     SPACE eurjchem-108 47 87 1h 1h NUM eurjchem-108 47 88 , , PUNCT eurjchem-108 47 89     SPACE eurjchem-108 47 90 h‐4 h‐4 NOUN eurjchem-108 47 91 ) ) PUNCT eurjchem-108 47 92 , , PUNCT eurjchem-108 47 93     SPACE eurjchem-108 47 94 6.69‐6.92 6.69‐6.92 NUM eurjchem-108 47 95     SPACE eurjchem-108 47 96 ( ( PUNCT eurjchem-108 47 97 m m PROPN eurjchem-108 47 98 , , PUNCT eurjchem-108 47 99     SPACE eurjchem-108 47 100 3h 3h NUM eurjchem-108 47 101 , , PUNCT eurjchem-108 47 102     SPACE eurjchem-108 47 103 ar‐h ar‐h NOUN eurjchem-108 47 104 ) ) PUNCT eurjchem-108 47 105 , , PUNCT eurjchem-108 47 106     SPACE eurjchem-108 47 107 9.65 9.65 NUM eurjchem-108 47 108     SPACE eurjchem-108 47 109 ( ( PUNCT eurjchem-108 47 110 s s PROPN eurjchem-108 47 111 , , PUNCT eurjchem-108 47 112         SPACE eurjchem-108 47 113 1h 1h NUM eurjchem-108 47 114 , , PUNCT eurjchem-108 47 115         SPACE eurjchem-108 47 116 n3‐h n3‐h PROPN eurjchem-108 47 117 ) ) PUNCT eurjchem-108 47 118 , , PUNCT eurjchem-108 47 119     SPACE eurjchem-108 47 120 10.55 10.55 NUM eurjchem-108 47 121     SPACE eurjchem-108 47 122 ( ( PUNCT eurjchem-108 47 123 s s PROPN eurjchem-108 47 124 , , PUNCT eurjchem-108 47 125         SPACE eurjchem-108 47 126 1h 1h NUM eurjchem-108 47 127 , , PUNCT eurjchem-108 47 128         SPACE eurjchem-108 47 129 n1‐h n1‐h PROPN eurjchem-108 47 130 ) ) PUNCT eurjchem-108 47 131 . . PUNCT eurjchem-108 47 132     SPACE eurjchem-108 48 1 anal anal ADJ eurjchem-108 48 2 . . PUNCT eurjchem-108 48 3     SPACE eurjchem-108 48 4 calcd calcd NOUN eurjchem-108 48 5 . . PUNCT eurjchem-108 48 6     SPACE eurjchem-108 48 7 for for ADP eurjchem-108 48 8     SPACE eurjchem-108 48 9 c18h22n2o3s c18h22n2o3s NUM eurjchem-108 48 10 : : PUNCT eurjchem-108 48 11     SPACE eurjchem-108 48 12 c c NOUN eurjchem-108 48 13 , , PUNCT eurjchem-108 48 14     SPACE eurjchem-108 48 15 68.40 68.40 NUM eurjchem-108 48 16 ; ; PUNCT eurjchem-108 48 17     SPACE eurjchem-108 48 18 h h NOUN eurjchem-108 48 19 , , PUNCT eurjchem-108 48 20     SPACE eurjchem-108 48 21 6.40 6.40 NUM eurjchem-108 48 22 ; ; PUNCT eurjchem-108 48 23     SPACE eurjchem-108 48 24 n n CCONJ eurjchem-108 48 25 , , PUNCT eurjchem-108 48 26     SPACE eurjchem-108 48 27 8.09 8.09 NUM eurjchem-108 48 28 % % NOUN eurjchem-108 48 29 . . PUNCT eurjchem-108 48 30     SPACE eurjchem-108 48 31 found find VERB eurjchem-108 48 32 : : PUNCT eurjchem-108 48 33     SPACE eurjchem-108 48 34 c c X eurjchem-108 48 35 , , PUNCT eurjchem-108 48 36     SPACE eurjchem-108 48 37 68.51 68.51 NUM eurjchem-108 48 38 ; ; PUNCT eurjchem-108 48 39     SPACE eurjchem-108 48 40 h h NOUN eurjchem-108 48 41 , , PUNCT eurjchem-108 48 42     SPACE eurjchem-108 48 43 6.32 6.32 NUM eurjchem-108 48 44 ; ; PUNCT eurjchem-108 48 45     SPACE eurjchem-108 48 46 n n CCONJ eurjchem-108 48 47 , , PUNCT eurjchem-108 48 48     SPACE eurjchem-108 48 49 8.20 8.20 NUM eurjchem-108 48 50 % % NOUN eurjchem-108 48 51 . . PUNCT eurjchem-108 48 52     SPACE eurjchem-108 49 1 4­(3­chlorophenyl)­7,7­dimethyl­5­oxo­1,2,3,4,5,6,7,8­ 4­(3­chlorophenyl)­7,7­dimethyl­5­oxo­1,2,3,4,5,6,7,8­ PROPN eurjchem-108 49 2 octahydroquinazoline­2­thione octahydroquinazoline­2­thione PROPN eurjchem-108 49 3     SPACE eurjchem-108 49 4 ( ( PUNCT eurjchem-108 49 5 4 4 NUM eurjchem-108 49 6 m m NUM eurjchem-108 49 7 ): ): PUNCT eurjchem-108 49 8     SPACE eurjchem-108 49 9 ir ir VERB eurjchem-108 49 10     SPACE eurjchem-108 49 11 ( ( PUNCT eurjchem-108 49 12 kbr kbr PROPN eurjchem-108 49 13 , , PUNCT eurjchem-108 49 14     SPACE eurjchem-108 49 15 cm‐1 cm‐1 NOUN eurjchem-108 49 16 ): ): PUNCT eurjchem-108 49 17     SPACE eurjchem-108 49 18 3237 3237 NUM eurjchem-108 49 19 , , PUNCT eurjchem-108 49 20     SPACE eurjchem-108 49 21 2954 2954 NUM eurjchem-108 49 22 , , PUNCT eurjchem-108 49 23     SPACE eurjchem-108 49 24 1623 1623 NUM eurjchem-108 49 25 , , PUNCT eurjchem-108 49 26     SPACE eurjchem-108 49 27 1577 1577 NUM eurjchem-108 49 28 , , PUNCT eurjchem-108 49 29     SPACE eurjchem-108 49 30 1459 1459 NUM eurjchem-108 49 31 . . PUNCT eurjchem-108 49 32     SPACE eurjchem-108 50 1 1h‐nmr 1h‐nmr NUM eurjchem-108 50 2     SPACE eurjchem-108 50 3 ( ( PUNCT eurjchem-108 50 4 dmso‐d6 dmso‐d6 PROPN eurjchem-108 50 5 , , PUNCT eurjchem-108 50 6     SPACE eurjchem-108 50 7 δ δ PROPN eurjchem-108 50 8 , , PUNCT eurjchem-108 50 9     SPACE eurjchem-108 50 10 ppm ppm NOUN eurjchem-108 50 11 ): ): PUNCT eurjchem-108 50 12     SPACE eurjchem-108 50 13 0.89 0.89 NUM eurjchem-108 50 14     SPACE eurjchem-108 50 15 ( ( PUNCT eurjchem-108 50 16 s s PROPN eurjchem-108 50 17 , , PUNCT eurjchem-108 50 18     SPACE eurjchem-108 50 19 3h 3h NUM eurjchem-108 50 20 , , PUNCT eurjchem-108 50 21     SPACE eurjchem-108 50 22 ch3 ch3 PROPN eurjchem-108 50 23 ) ) PUNCT eurjchem-108 50 24 , , PUNCT eurjchem-108 50 25     SPACE eurjchem-108 50 26 1.02 1.02 NUM eurjchem-108 50 27     SPACE eurjchem-108 50 28 ( ( PUNCT eurjchem-108 50 29 s s PROPN eurjchem-108 50 30 , , PUNCT eurjchem-108 50 31     SPACE eurjchem-108 50 32 3h 3h NUM eurjchem-108 50 33 , , PUNCT eurjchem-108 50 34     SPACE eurjchem-108 50 35 ch3 ch3 PROPN eurjchem-108 50 36 ) ) PUNCT eurjchem-108 50 37 , , PUNCT eurjchem-108 50 38     SPACE eurjchem-108 50 39 2.06‐2.42 2.06‐2.42 NUM eurjchem-108 50 40     SPACE eurjchem-108 50 41 ( ( PUNCT eurjchem-108 50 42 m m PROPN eurjchem-108 50 43 , , PUNCT eurjchem-108 50 44     SPACE eurjchem-108 50 45 4h 4h NOUN eurjchem-108 50 46 , , PUNCT eurjchem-108 50 47     SPACE eurjchem-108 50 48 ch2‐8 ch2‐8 PROPN eurjchem-108 50 49 , , PUNCT eurjchem-108 50 50     SPACE eurjchem-108 50 51 ch2‐6 ch2‐6 NOUN eurjchem-108 50 52 ) ) PUNCT eurjchem-108 50 53 , , PUNCT eurjchem-108 50 54     SPACE eurjchem-108 50 55 5.19 5.19 NUM eurjchem-108 50 56     SPACE eurjchem-108 50 57 ( ( PUNCT eurjchem-108 50 58 d d PROPN eurjchem-108 50 59 , , PUNCT eurjchem-108 50 60     SPACE eurjchem-108 50 61 j=3.12 j=3.12 NOUN eurjchem-108 50 62     SPACE eurjchem-108 50 63 hz hz VERB eurjchem-108 50 64 , , PUNCT eurjchem-108 50 65     SPACE eurjchem-108 50 66 1h 1h NUM eurjchem-108 50 67 , , PUNCT eurjchem-108 50 68     SPACE eurjchem-108 50 69 h‐4 h‐4 NOUN eurjchem-108 50 70 ) ) PUNCT eurjchem-108 50 71 , , PUNCT eurjchem-108 50 72     SPACE eurjchem-108 50 73 7.16‐7.42 7.16‐7.42 NUM eurjchem-108 50 74     SPACE eurjchem-108 50 75 ( ( PUNCT eurjchem-108 50 76 m m PROPN eurjchem-108 50 77 , , PUNCT eurjchem-108 50 78     SPACE eurjchem-108 50 79 4h 4h NOUN eurjchem-108 50 80 , , PUNCT eurjchem-108 50 81     SPACE eurjchem-108 50 82 ar‐h ar‐h NOUN eurjchem-108 50 83 ) ) PUNCT eurjchem-108 50 84 , , PUNCT eurjchem-108 50 85     SPACE eurjchem-108 50 86 9.73 9.73 NUM eurjchem-108 50 87     SPACE eurjchem-108 50 88 ( ( PUNCT eurjchem-108 50 89 s s PROPN eurjchem-108 50 90 , , PUNCT eurjchem-108 50 91       SPACE eurjchem-108 50 92 1h 1h NUM eurjchem-108 50 93 , , PUNCT eurjchem-108 50 94       SPACE eurjchem-108 50 95 n3‐h n3‐h PROPN eurjchem-108 50 96 ) ) PUNCT eurjchem-108 50 97 , , PUNCT eurjchem-108 50 98     SPACE eurjchem-108 50 99 10.68 10.68 NUM eurjchem-108 50 100     SPACE eurjchem-108 50 101 ( ( PUNCT eurjchem-108 50 102 s s PROPN eurjchem-108 50 103 , , PUNCT eurjchem-108 50 104       SPACE eurjchem-108 50 105 1h 1h NUM eurjchem-108 50 106 , , PUNCT eurjchem-108 50 107       SPACE eurjchem-108 50 108 n1‐h n1‐h PROPN eurjchem-108 50 109 ) ) PUNCT eurjchem-108 50 110 . . PUNCT eurjchem-108 50 111     SPACE eurjchem-108 51 1 anal anal ADJ eurjchem-108 51 2 . . PUNCT eurjchem-108 51 3     SPACE eurjchem-108 51 4 calcd calcd NOUN eurjchem-108 51 5 . . PUNCT eurjchem-108 51 6     SPACE eurjchem-108 51 7 for for ADP eurjchem-108 51 8     SPACE eurjchem-108 51 9 c16h17cln2os c16h17cln2o NOUN eurjchem-108 51 10 : : PUNCT eurjchem-108 51 11     SPACE eurjchem-108 51 12 c c X eurjchem-108 51 13 , , PUNCT eurjchem-108 51 14     SPACE eurjchem-108 51 15 59.90 59.90 NUM eurjchem-108 51 16 ; ; PUNCT eurjchem-108 51 17     SPACE eurjchem-108 51 18 h h NOUN eurjchem-108 51 19 , , PUNCT eurjchem-108 51 20     SPACE eurjchem-108 51 21 5.34 5.34 NUM eurjchem-108 51 22 ; ; PUNCT eurjchem-108 51 23     SPACE eurjchem-108 51 24 n n CCONJ eurjchem-108 51 25 , , PUNCT eurjchem-108 51 26     SPACE eurjchem-108 51 27 8.73 8.73 NUM eurjchem-108 51 28 % % NOUN eurjchem-108 51 29 . . PUNCT eurjchem-108 51 30     SPACE eurjchem-108 51 31 found find VERB eurjchem-108 51 32 : : PUNCT eurjchem-108 51 33     SPACE eurjchem-108 51 34 c c X eurjchem-108 51 35 , , PUNCT eurjchem-108 51 36     SPACE eurjchem-108 51 37 59.72 59.72 NUM eurjchem-108 51 38 ; ; PUNCT eurjchem-108 51 39     SPACE eurjchem-108 51 40 h h NOUN eurjchem-108 51 41 , , PUNCT eurjchem-108 51 42     SPACE eurjchem-108 51 43 5.41 5.41 NUM eurjchem-108 51 44 ; ; PUNCT eurjchem-108 51 45     SPACE eurjchem-108 51 46 n n CCONJ eurjchem-108 51 47 , , PUNCT eurjchem-108 51 48     SPACE eurjchem-108 51 49 8.75 8.75 NUM eurjchem-108 51 50 % % NOUN eurjchem-108 51 51 . . PUNCT eurjchem-108 51 52         SPACE eurjchem-108 52 1 3 3 NUM eurjchem-108 52 2 . . PUNCT eurjchem-108 52 3     SPACE eurjchem-108 52 4 results result VERB eurjchem-108 52 5     SPACE eurjchem-108 52 6 and and CCONJ eurjchem-108 52 7     SPACE eurjchem-108 52 8 discussion discussion NOUN eurjchem-108 52 9         SPACE eurjchem-108 52 10 dihydropyrimidinones dihydropyrimidinone NOUN eurjchem-108 52 11 , , PUNCT eurjchem-108 52 12     SPACE eurjchem-108 52 13 4a­o 4a­o PROPN eurjchem-108 52 14     SPACE eurjchem-108 52 15 were be AUX eurjchem-108 52 16     SPACE eurjchem-108 52 17 synthesized synthesize VERB eurjchem-108 52 18     SPACE eurjchem-108 52 19 by by ADP eurjchem-108 52 20     SPACE eurjchem-108 52 21 reaction reaction NOUN eurjchem-108 52 22     SPACE eurjchem-108 52 23 of of ADP eurjchem-108 52 24     SPACE eurjchem-108 52 25 5,5‐dimethyl‐1,3‐hexadion 5,5‐dimethyl‐1,3‐hexadion NOUN eurjchem-108 52 26     SPACE eurjchem-108 52 27 ( ( PUNCT eurjchem-108 52 28 dimedone dimedone NOUN eurjchem-108 52 29 ) ) PUNCT eurjchem-108 52 30     SPACE eurjchem-108 52 31 and and CCONJ eurjchem-108 52 32     SPACE eurjchem-108 52 33 corresponding corresponding ADJ eurjchem-108 52 34     SPACE eurjchem-108 52 35 aromatic aromatic ADJ eurjchem-108 52 36     SPACE eurjchem-108 52 37 aldehyde aldehyde NOUN eurjchem-108 52 38     SPACE eurjchem-108 52 39 with with ADP eurjchem-108 52 40     SPACE eurjchem-108 52 41 urea urea NOUN eurjchem-108 52 42     SPACE eurjchem-108 52 43 ( ( PUNCT eurjchem-108 52 44 or or CCONJ eurjchem-108 52 45     SPACE eurjchem-108 52 46 thiourea thiourea NOUN eurjchem-108 52 47 ) ) PUNCT eurjchem-108 52 48     SPACE eurjchem-108 52 49 in in ADP eurjchem-108 52 50     SPACE eurjchem-108 52 51 the the DET eurjchem-108 52 52     SPACE eurjchem-108 52 53 presence presence NOUN eurjchem-108 52 54     SPACE eurjchem-108 52 55 of of ADP eurjchem-108 52 56     SPACE eurjchem-108 52 57 catalytic catalytic ADJ eurjchem-108 52 58     SPACE eurjchem-108 52 59 amount amount NOUN eurjchem-108 52 60     SPACE eurjchem-108 52 61 of of ADP eurjchem-108 52 62     SPACE eurjchem-108 52 63 silica silica NOUN eurjchem-108 52 64     SPACE eurjchem-108 52 65 sulfuric sulfuric NOUN eurjchem-108 52 66     SPACE eurjchem-108 52 67 acid acid NOUN eurjchem-108 52 68     SPACE eurjchem-108 52 69 in in ADP eurjchem-108 52 70     SPACE eurjchem-108 52 71 refluxing refluxing NOUN eurjchem-108 52 72     SPACE eurjchem-108 52 73 ethanol ethanol NOUN eurjchem-108 52 74     SPACE eurjchem-108 52 75 ( ( PUNCT eurjchem-108 52 76 scheme scheme NOUN eurjchem-108 52 77     SPACE eurjchem-108 52 78 1 1 NUM eurjchem-108 52 79 ) ) PUNCT eurjchem-108 52 80 . . PUNCT eurjchem-108 52 81     SPACE eurjchem-108 53 1 the the DET eurjchem-108 53 2     SPACE eurjchem-108 53 3 yield yield NOUN eurjchem-108 53 4     SPACE eurjchem-108 53 5 of of ADP eurjchem-108 53 6     SPACE eurjchem-108 53 7 products product NOUN eurjchem-108 53 8     SPACE eurjchem-108 53 9 was be AUX eurjchem-108 53 10     SPACE eurjchem-108 53 11 good good ADJ eurjchem-108 53 12     SPACE eurjchem-108 53 13 to to ADP eurjchem-108 53 14     SPACE eurjchem-108 53 15 excellent excellent ADJ eurjchem-108 53 16     SPACE eurjchem-108 53 17 without without ADP eurjchem-108 53 18     SPACE eurjchem-108 53 19 the the DET eurjchem-108 53 20     SPACE eurjchem-108 53 21 formation formation NOUN eurjchem-108 53 22     SPACE eurjchem-108 53 23 of of ADP eurjchem-108 53 24     SPACE eurjchem-108 53 25 1,8‐dioxo‐octahydoxanthenes 1,8‐dioxo‐octahydoxanthenes NUM eurjchem-108 53 26     SPACE eurjchem-108 53 27 5 5 NUM eurjchem-108 53 28 , , PUNCT eurjchem-108 53 29     SPACE eurjchem-108 53 30 which which PRON eurjchem-108 53 31     SPACE eurjchem-108 53 32 is be AUX eurjchem-108 53 33     SPACE eurjchem-108 53 34 the the DET eurjchem-108 53 35     SPACE eurjchem-108 53 36 major major ADJ eurjchem-108 53 37     SPACE eurjchem-108 53 38 product product NOUN eurjchem-108 53 39     SPACE eurjchem-108 53 40 of of ADP eurjchem-108 53 41     SPACE eurjchem-108 53 42 the the DET eurjchem-108 53 43     SPACE eurjchem-108 53 44 procedure procedure NOUN eurjchem-108 53 45     SPACE eurjchem-108 53 46 reported report VERB eurjchem-108 53 47     SPACE eurjchem-108 53 48 by by ADP eurjchem-108 53 49     SPACE eurjchem-108 53 50 the the DET eurjchem-108 53 51     SPACE eurjchem-108 53 52 literature literature NOUN eurjchem-108 53 53     SPACE eurjchem-108 54 1 [ [ X eurjchem-108 54 2 22 22 NUM eurjchem-108 54 3 ] ] PUNCT eurjchem-108 54 4 . . PUNCT eurjchem-108 54 5     SPACE eurjchem-108 55 1 the the DET eurjchem-108 55 2     SPACE eurjchem-108 55 3 reaction reaction NOUN eurjchem-108 55 4     SPACE eurjchem-108 55 5 did do AUX eurjchem-108 55 6     SPACE eurjchem-108 55 7 not not PART eurjchem-108 55 8     SPACE eurjchem-108 55 9 proceed proceed VERB eurjchem-108 55 10     SPACE eurjchem-108 55 11 in in ADP eurjchem-108 55 12     SPACE eurjchem-108 55 13 the the DET eurjchem-108 55 14     SPACE eurjchem-108 55 15 absence absence NOUN eurjchem-108 55 16     SPACE eurjchem-108 55 17 of of ADP eurjchem-108 55 18     SPACE eurjchem-108 55 19 ssa ssa NOUN eurjchem-108 55 20     SPACE eurjchem-108 55 21 after after ADP eurjchem-108 55 22     SPACE eurjchem-108 55 23 long long ADJ eurjchem-108 55 24     SPACE eurjchem-108 55 25 reaction reaction NOUN eurjchem-108 55 26     SPACE eurjchem-108 55 27 times time NOUN eurjchem-108 55 28 . . PUNCT eurjchem-108 55 29     SPACE eurjchem-108 56 1 the the DET eurjchem-108 56 2     SPACE eurjchem-108 56 3 results result NOUN eurjchem-108 56 4     SPACE eurjchem-108 56 5 are be AUX eurjchem-108 56 6     SPACE eurjchem-108 56 7 summarized summarize VERB eurjchem-108 56 8     SPACE eurjchem-108 56 9 in in ADP eurjchem-108 56 10     SPACE eurjchem-108 56 11 table table NOUN eurjchem-108 56 12     SPACE eurjchem-108 56 13 1 1 NUM eurjchem-108 56 14 . . PUNCT eurjchem-108 56 15     SPACE eurjchem-108 56 16 in in ADP eurjchem-108 56 17     SPACE eurjchem-108 56 18 view view NOUN eurjchem-108 56 19     SPACE eurjchem-108 56 20 of of ADP eurjchem-108 56 21     SPACE eurjchem-108 56 22 environmentally environmentally ADV eurjchem-108 56 23     SPACE eurjchem-108 56 24 friendly friendly ADJ eurjchem-108 56 25     SPACE eurjchem-108 56 26 procedure procedure NOUN eurjchem-108 56 27 , , PUNCT eurjchem-108 56 28     SPACE eurjchem-108 56 29 the the DET eurjchem-108 56 30     SPACE eurjchem-108 56 31 recovery recovery NOUN eurjchem-108 56 32     SPACE eurjchem-108 56 33 and and CCONJ eurjchem-108 56 34     SPACE eurjchem-108 56 35 reuse reuse NOUN eurjchem-108 56 36     SPACE eurjchem-108 56 37 of of ADP eurjchem-108 56 38     SPACE eurjchem-108 56 39 this this DET eurjchem-108 56 40     SPACE eurjchem-108 56 41 catalyst catalyst NOUN eurjchem-108 56 42     SPACE eurjchem-108 56 43 is be AUX eurjchem-108 56 44     SPACE eurjchem-108 56 45 quite quite ADV eurjchem-108 56 46     SPACE eurjchem-108 56 47 preferable preferable ADJ eurjchem-108 56 48 . . PUNCT eurjchem-108 56 49     SPACE eurjchem-108 56 50 silica silica NOUN eurjchem-108 56 51     SPACE eurjchem-108 56 52 sulfuric sulfuric NOUN eurjchem-108 56 53     SPACE eurjchem-108 56 54 acid acid NOUN eurjchem-108 56 55     SPACE eurjchem-108 56 56 was be AUX eurjchem-108 56 57     SPACE eurjchem-108 56 58 easily easily ADV eurjchem-108 56 59     SPACE eurjchem-108 56 60 separated separate VERB eurjchem-108 56 61     SPACE eurjchem-108 56 62 from from ADP eurjchem-108 56 63     SPACE eurjchem-108 56 64 the the DET eurjchem-108 56 65     SPACE eurjchem-108 56 66 reaction reaction NOUN eurjchem-108 56 67     SPACE eurjchem-108 56 68 medium medium NOUN eurjchem-108 56 69     SPACE eurjchem-108 56 70 by by ADP eurjchem-108 56 71     SPACE eurjchem-108 56 72 filtering filtering NOUN eurjchem-108 56 73     SPACE eurjchem-108 56 74 and and CCONJ eurjchem-108 56 75     SPACE eurjchem-108 56 76 regenerated regenerate VERB eurjchem-108 56 77     SPACE eurjchem-108 56 78 by by ADP eurjchem-108 56 79     SPACE eurjchem-108 56 80 washing washing NOUN eurjchem-108 56 81     SPACE eurjchem-108 56 82 with with ADP eurjchem-108 56 83     SPACE eurjchem-108 56 84 water water NOUN eurjchem-108 56 85     SPACE eurjchem-108 56 86 and and CCONJ eurjchem-108 56 87     SPACE eurjchem-108 56 88 ethanol ethanol NOUN eurjchem-108 56 89 , , PUNCT eurjchem-108 56 90     SPACE eurjchem-108 56 91 followed follow VERB eurjchem-108 56 92     SPACE eurjchem-108 56 93 by by ADP eurjchem-108 56 94     SPACE eurjchem-108 56 95 drying dry VERB eurjchem-108 56 96     SPACE eurjchem-108 56 97 at at ADP eurjchem-108 56 98     SPACE eurjchem-108 56 99 room room NOUN eurjchem-108 56 100     SPACE eurjchem-108 56 101 temperature temperature NOUN eurjchem-108 56 102 . . PUNCT eurjchem-108 56 103     SPACE eurjchem-108 57 1 the the DET eurjchem-108 57 2     SPACE eurjchem-108 57 3 catalyst catalyst NOUN eurjchem-108 57 4     SPACE eurjchem-108 57 5 was be AUX eurjchem-108 57 6     SPACE eurjchem-108 57 7 reused reuse VERB eurjchem-108 57 8     SPACE eurjchem-108 57 9 three three NUM eurjchem-108 57 10     SPACE eurjchem-108 57 11 times time NOUN eurjchem-108 57 12     SPACE eurjchem-108 57 13 for for ADP eurjchem-108 57 14     SPACE eurjchem-108 57 15 preparation preparation NOUN eurjchem-108 57 16     SPACE eurjchem-108 57 17 of of ADP eurjchem-108 57 18     SPACE eurjchem-108 57 19 4i 4i NOUN eurjchem-108 57 20 , , PUNCT eurjchem-108 57 21     SPACE eurjchem-108 57 22 as as ADP eurjchem-108 57 23     SPACE eurjchem-108 57 24 a a DET eurjchem-108 57 25     SPACE eurjchem-108 57 26 model model NOUN eurjchem-108 57 27     SPACE eurjchem-108 57 28 reaction reaction NOUN eurjchem-108 57 29 , , PUNCT eurjchem-108 57 30     SPACE eurjchem-108 57 31 without without ADP eurjchem-108 57 32     SPACE eurjchem-108 57 33 significant significant ADJ eurjchem-108 57 34     SPACE eurjchem-108 57 35 loose loose ADJ eurjchem-108 57 36     SPACE eurjchem-108 57 37 of of ADP eurjchem-108 57 38     SPACE eurjchem-108 57 39 activity activity NOUN eurjchem-108 57 40     SPACE eurjchem-108 57 41 ( ( PUNCT eurjchem-108 57 42 table table NOUN eurjchem-108 57 43     SPACE eurjchem-108 57 44 1 1 NUM eurjchem-108 57 45 ) ) PUNCT eurjchem-108 57 46 . . PUNCT eurjchem-108 57 47     SPACE eurjchem-108 58 1 among among ADP eurjchem-108 58 2     SPACE eurjchem-108 58 3 the the DET eurjchem-108 58 4     SPACE eurjchem-108 58 5 various various ADJ eurjchem-108 58 6     SPACE eurjchem-108 58 7 acid acid NOUN eurjchem-108 58 8     SPACE eurjchem-108 58 9 catalysts catalyst NOUN eurjchem-108 58 10     SPACE eurjchem-108 58 11 used use VERB eurjchem-108 58 12     SPACE eurjchem-108 58 13 for for ADP eurjchem-108 58 14     SPACE eurjchem-108 58 15 preparation preparation NOUN eurjchem-108 58 16     SPACE eurjchem-108 58 17 of of ADP eurjchem-108 58 18     SPACE eurjchem-108 58 19 octahydro octahydro NOUN eurjchem-108 58 20     SPACE eurjchem-108 58 21 quinazolinones quinazolinone NOUN eurjchem-108 58 22     SPACE eurjchem-108 59 1 [ [ X eurjchem-108 59 2 9‐13,23 9‐13,23 NOUN eurjchem-108 59 3 ] ] X eurjchem-108 59 4 , , PUNCT eurjchem-108 59 5     SPACE eurjchem-108 59 6 the the DET eurjchem-108 59 7     SPACE eurjchem-108 59 8 silica silica NOUN eurjchem-108 59 9     SPACE eurjchem-108 59 10 sulfuric sulfuric NOUN eurjchem-108 59 11     SPACE eurjchem-108 59 12 acid acid NOUN eurjchem-108 59 13     SPACE eurjchem-108 59 14 was be AUX eurjchem-108 59 15     SPACE eurjchem-108 59 16 found find VERB eurjchem-108 59 17     SPACE eurjchem-108 59 18 more more ADV eurjchem-108 59 19     SPACE eurjchem-108 59 20 preferable preferable ADJ eurjchem-108 59 21     SPACE eurjchem-108 59 22 catalyst catalyst NOUN eurjchem-108 59 23     SPACE eurjchem-108 59 24 because because SCONJ eurjchem-108 59 25     SPACE eurjchem-108 59 26 of of ADP eurjchem-108 59 27     SPACE eurjchem-108 59 28 its its PRON eurjchem-108 59 29     SPACE eurjchem-108 59 30 suitable suitable ADJ eurjchem-108 59 31     SPACE eurjchem-108 59 32 acidity acidity NOUN eurjchem-108 59 33 , , PUNCT eurjchem-108 59 34     SPACE eurjchem-108 59 35 availability availability NOUN eurjchem-108 59 36     SPACE eurjchem-108 59 37 and and CCONJ eurjchem-108 59 38     SPACE eurjchem-108 59 39 low low ADJ eurjchem-108 59 40     SPACE eurjchem-108 59 41 cost cost NOUN eurjchem-108 59 42 . . PUNCT eurjchem-108 59 43     SPACE eurjchem-108 60 1 yields yield NOUN eurjchem-108 60 2     SPACE eurjchem-108 60 3 of of ADP eurjchem-108 60 4     SPACE eurjchem-108 60 5 this this DET eurjchem-108 60 6     SPACE eurjchem-108 60 7 one‐pot one‐pot NOUN eurjchem-108 60 8     SPACE eurjchem-108 60 9 protocol protocol NOUN eurjchem-108 60 10     SPACE eurjchem-108 60 11 reactions reaction NOUN eurjchem-108 60 12     SPACE eurjchem-108 60 13 following follow VERB eurjchem-108 60 14     SPACE eurjchem-108 60 15 recrystallization recrystallization NOUN eurjchem-108 60 16     SPACE eurjchem-108 60 17 from from ADP eurjchem-108 60 18     SPACE eurjchem-108 60 19 ethanol ethanol NOUN eurjchem-108 60 20     SPACE eurjchem-108 60 21 were be AUX eurjchem-108 60 22     SPACE eurjchem-108 60 23 of of ADP eurjchem-108 60 24     SPACE eurjchem-108 60 25 the the DET eurjchem-108 60 26     SPACE eurjchem-108 60 27 order order NOUN eurjchem-108 60 28     SPACE eurjchem-108 60 29 76‐93 76‐93 NUM eurjchem-108 60 30 % % NOUN eurjchem-108 60 31 , , PUNCT eurjchem-108 60 32     SPACE eurjchem-108 60 33 which which PRON eurjchem-108 60 34     SPACE eurjchem-108 60 35 is be AUX eurjchem-108 60 36     SPACE eurjchem-108 60 37 very very ADV eurjchem-108 60 38     SPACE eurjchem-108 60 39 favorable favorable ADJ eurjchem-108 60 40     SPACE eurjchem-108 60 41 as as ADP eurjchem-108 60 42     SPACE eurjchem-108 60 43 compared compare VERB eurjchem-108 60 44     SPACE eurjchem-108 60 45 with with ADP eurjchem-108 60 46     SPACE eurjchem-108 60 47 other other ADJ eurjchem-108 60 48     SPACE eurjchem-108 60 49 procedures procedure NOUN eurjchem-108 60 50     SPACE eurjchem-108 60 51 ( ( PUNCT eurjchem-108 60 52 46‐98 46‐98 NUM eurjchem-108 60 53 % % NOUN eurjchem-108 60 54 ) ) PUNCT eurjchem-108 60 55     SPACE eurjchem-108 61 1 [ [ X eurjchem-108 61 2 8,22 8,22 NUM eurjchem-108 61 3 ] ] X eurjchem-108 61 4 . . PUNCT eurjchem-108 61 5     SPACE eurjchem-108 61 6 all all PRON eurjchem-108 61 7     SPACE eurjchem-108 61 8 obtained obtain VERB eurjchem-108 61 9     SPACE eurjchem-108 61 10 products product NOUN eurjchem-108 61 11     SPACE eurjchem-108 61 12 were be AUX eurjchem-108 61 13     SPACE eurjchem-108 61 14 characterized characterize VERB eurjchem-108 61 15     SPACE eurjchem-108 61 16 by by ADP eurjchem-108 61 17     SPACE eurjchem-108 61 18 nmr nmr NOUN eurjchem-108 61 19     SPACE eurjchem-108 61 20 and and CCONJ eurjchem-108 61 21     SPACE eurjchem-108 61 22 ir ir PROPN eurjchem-108 61 23     SPACE eurjchem-108 61 24 spectra spectra NOUN eurjchem-108 61 25     SPACE eurjchem-108 61 26 as as ADV eurjchem-108 61 27     SPACE eurjchem-108 61 28 well well ADV eurjchem-108 61 29     SPACE eurjchem-108 61 30 as as ADP eurjchem-108 61 31     SPACE eurjchem-108 61 32 their their PRON eurjchem-108 61 33     SPACE eurjchem-108 61 34 elemental elemental ADJ eurjchem-108 61 35     SPACE eurjchem-108 61 36 analysis analysis NOUN eurjchem-108 61 37     SPACE eurjchem-108 61 38 data datum NOUN eurjchem-108 61 39 . . PUNCT eurjchem-108 61 40     SPACE eurjchem-108 61 41 in in ADP eurjchem-108 61 42     SPACE eurjchem-108 61 43 the the DET eurjchem-108 61 44     SPACE eurjchem-108 61 45 1h‐ 1h‐ NUM eurjchem-108 61 46 nmr nmr NOUN eurjchem-108 61 47     SPACE eurjchem-108 61 48 spectra spectra NOUN eurjchem-108 61 49     SPACE eurjchem-108 61 50 of of ADP eurjchem-108 61 51     SPACE eurjchem-108 61 52 these these PRON eurjchem-108 61 53     SPACE eurjchem-108 61 54 compounds compound VERB eurjchem-108 61 55     SPACE eurjchem-108 61 56 the the DET eurjchem-108 61 57     SPACE eurjchem-108 61 58 two two NUM eurjchem-108 61 59     SPACE eurjchem-108 61 60 different different ADJ eurjchem-108 61 61     SPACE eurjchem-108 61 62 broad broad ADJ eurjchem-108 61 63     SPACE eurjchem-108 61 64 signals signal NOUN eurjchem-108 61 65     SPACE eurjchem-108 61 66 at at ADP eurjchem-108 61 67     SPACE eurjchem-108 61 68 low low ADJ eurjchem-108 61 69     SPACE eurjchem-108 61 70 field field NOUN eurjchem-108 61 71     SPACE eurjchem-108 61 72 were be AUX eurjchem-108 61 73     SPACE eurjchem-108 61 74 assigned assign VERB eurjchem-108 61 75     SPACE eurjchem-108 61 76 to to ADP eurjchem-108 61 77     SPACE eurjchem-108 61 78 the the DET eurjchem-108 61 79     SPACE eurjchem-108 61 80 resonance resonance NOUN eurjchem-108 61 81     SPACE eurjchem-108 61 82 of of ADP eurjchem-108 61 83     SPACE eurjchem-108 61 84 two two NUM eurjchem-108 61 85     SPACE eurjchem-108 61 86 nhs nhs NOUN eurjchem-108 61 87     SPACE eurjchem-108 61 88 protons proton NOUN eurjchem-108 61 89     SPACE eurjchem-108 61 90 of of ADP eurjchem-108 61 91     SPACE eurjchem-108 61 92 the the DET eurjchem-108 61 93     SPACE eurjchem-108 61 94 pyrimidine pyrimidine NOUN eurjchem-108 61 95     SPACE eurjchem-108 61 96 ring ring NOUN eurjchem-108 61 97 . . PUNCT eurjchem-108 61 98     SPACE eurjchem-108 62 1 this this PRON eurjchem-108 62 2     SPACE eurjchem-108 62 3 was be AUX eurjchem-108 62 4     SPACE eurjchem-108 62 5 supported support VERB eurjchem-108 62 6     SPACE eurjchem-108 62 7 by by ADP eurjchem-108 62 8     SPACE eurjchem-108 62 9 ir ir PROPN eurjchem-108 62 10     SPACE eurjchem-108 62 11 spectra spectra NOUN eurjchem-108 62 12 , , PUNCT eurjchem-108 62 13     SPACE eurjchem-108 62 14 which which PRON eurjchem-108 62 15     SPACE eurjchem-108 62 16 included include VERB eurjchem-108 62 17     SPACE eurjchem-108 62 18 signals signal NOUN eurjchem-108 62 19     SPACE eurjchem-108 62 20 in in ADP eurjchem-108 62 21     SPACE eurjchem-108 62 22 the the DET eurjchem-108 62 23     SPACE eurjchem-108 62 24 region region NOUN eurjchem-108 62 25     SPACE eurjchem-108 62 26 3165‐3285 3165‐3285 NUM eurjchem-108 62 27     SPACE eurjchem-108 62 28 cm‐1 cm‐1 PROPN eurjchem-108 62 29 . . PUNCT eurjchem-108 62 30             SPACE eurjchem-108 63 1 mobinikhaledi mobinikhaledi PROPN eurjchem-108 63 2     SPACE eurjchem-108 63 3 et et PROPN eurjchem-108 63 4     SPACE eurjchem-108 63 5 al al PROPN eurjchem-108 63 6 . . PROPN eurjchem-108 63 7     SPACE eurjchem-108 63 8 / / SYM eurjchem-108 63 9     SPACE eurjchem-108 63 10 european european ADJ eurjchem-108 63 11     SPACE eurjchem-108 63 12 journal journal NOUN eurjchem-108 63 13     SPACE eurjchem-108 63 14 of of ADP eurjchem-108 63 15     SPACE eurjchem-108 63 16 chemistry chemistry NOUN eurjchem-108 63 17     SPACE eurjchem-108 63 18 1 1 NUM eurjchem-108 63 19     SPACE eurjchem-108 63 20 ( ( PUNCT eurjchem-108 63 21 4 4 NUM eurjchem-108 63 22 ) ) PUNCT eurjchem-108 63 23     SPACE eurjchem-108 63 24 ( ( PUNCT eurjchem-108 63 25 2010 2010 NUM eurjchem-108 63 26 ) ) PUNCT eurjchem-108 63 27     SPACE eurjchem-108 63 28 291­293 291­293 NUM eurjchem-108 63 29     SPACE eurjchem-108 63 30 293 293 NUM eurjchem-108 63 31         SPACE eurjchem-108 63 32 table table NOUN eurjchem-108 63 33     SPACE eurjchem-108 63 34 1 1 NUM eurjchem-108 63 35 . . PUNCT eurjchem-108 63 36       SPACE eurjchem-108 63 37 synthesis synthesis NOUN eurjchem-108 63 38     SPACE eurjchem-108 63 39 of of ADP eurjchem-108 63 40     SPACE eurjchem-108 63 41 octahydroquinazolinone octahydroquinazolinone NOUN eurjchem-108 63 42     SPACE eurjchem-108 63 43 derivatives derivative NOUN eurjchem-108 63 44     SPACE eurjchem-108 63 45 using use VERB eurjchem-108 63 46     SPACE eurjchem-108 63 47 ssa ssa NOUN eurjchem-108 63 48 . . PUNCT eurjchem-108 63 49     SPACE eurjchem-108 63 50 product product NOUN eurjchem-108 63 51     SPACE eurjchem-108 63 52 ( ( PUNCT eurjchem-108 63 53 4 4 NUM eurjchem-108 63 54 ) ) PUNCT eurjchem-108 63 55     SPACE eurjchem-108 63 56 x x NOUN eurjchem-108 63 57     SPACE eurjchem-108 63 58 r r NOUN eurjchem-108 63 59     SPACE eurjchem-108 63 60 time time NOUN eurjchem-108 63 61     SPACE eurjchem-108 63 62 ( ( PUNCT eurjchem-108 63 63 h h NOUN eurjchem-108 63 64 ) ) PUNCT eurjchem-108 63 65     SPACE eurjchem-108 63 66 yield yield NOUN eurjchem-108 63 67     SPACE eurjchem-108 63 68 ( ( PUNCT eurjchem-108 63 69 % % NOUN eurjchem-108 63 70 ) ) PUNCT eurjchem-108 63 71 / / SYM eurjchem-108 63 72     SPACE eurjchem-108 63 73 ( ( PUNCT eurjchem-108 63 74 lit light VERB eurjchem-108 63 75 . . PUNCT eurjchem-108 63 76 ) ) PUNCT eurjchem-108 63 77     SPACE eurjchem-108 64 1 m.p m.p PROPN eurjchem-108 64 2 . . PROPN eurjchem-108 64 3     SPACE eurjchem-108 64 4 ( ( PUNCT eurjchem-108 64 5 c)/ c)/ X eurjchem-108 64 6     SPACE eurjchem-108 64 7 ( ( PUNCT eurjchem-108 64 8 lit light VERB eurjchem-108 64 9 . . PUNCT eurjchem-108 64 10 ) ) PUNCT eurjchem-108 64 11     SPACE eurjchem-108 65 1 a a DET eurjchem-108 65 2     SPACE eurjchem-108 65 3 o o NOUN eurjchem-108 65 4     SPACE eurjchem-108 65 5 h h NOUN eurjchem-108 65 6     SPACE eurjchem-108 65 7 4 4 NUM eurjchem-108 65 8     SPACE eurjchem-108 65 9 90/(73 90/(73 NUM eurjchem-108 65 10 ) ) PUNCT eurjchem-108 65 11     SPACE eurjchem-108 66 1 [ [ X eurjchem-108 66 2 22 22 NUM eurjchem-108 66 3 ] ] PUNCT eurjchem-108 66 4     SPACE eurjchem-108 66 5 285‐286/(287‐290 285‐286/(287‐290 NUM eurjchem-108 66 6 ) ) PUNCT eurjchem-108 66 7     SPACE eurjchem-108 67 1 [ [ X eurjchem-108 67 2 22 22 NUM eurjchem-108 67 3 ] ] PUNCT eurjchem-108 67 4     SPACE eurjchem-108 67 5 b b NOUN eurjchem-108 67 6     SPACE eurjchem-108 67 7 o o NOUN eurjchem-108 67 8     SPACE eurjchem-108 67 9 4‐ch3 4‐ch3 ADJ eurjchem-108 67 10     SPACE eurjchem-108 67 11 3 3 NUM eurjchem-108 67 12     SPACE eurjchem-108 67 13 87/(39 87/(39 NUM eurjchem-108 67 14 ) ) PUNCT eurjchem-108 67 15     SPACE eurjchem-108 68 1 [ [ X eurjchem-108 68 2 3 3 NUM eurjchem-108 68 3 ] ] SYM eurjchem-108 68 4     SPACE eurjchem-108 68 5 319/ 319/ NUM eurjchem-108 68 6     SPACE eurjchem-108 68 7 ( ( PUNCT eurjchem-108 68 8 > > X eurjchem-108 68 9 300 300 NUM eurjchem-108 68 10 ) ) PUNCT eurjchem-108 68 11     SPACE eurjchem-108 69 1 [ [ X eurjchem-108 69 2 3 3 NUM eurjchem-108 69 3 ] ] PUNCT eurjchem-108 69 4     SPACE eurjchem-108 69 5 c c NOUN eurjchem-108 69 6     SPACE eurjchem-108 69 7 o o NOUN eurjchem-108 69 8     SPACE eurjchem-108 69 9 3,4‐(och3)2 3,4‐(och3)2 NUM eurjchem-108 69 10     SPACE eurjchem-108 69 11 9 9 NUM eurjchem-108 69 12     SPACE eurjchem-108 69 13 82 82 NUM eurjchem-108 69 14 268‐270 268‐270 NUM eurjchem-108 69 15     SPACE eurjchem-108 69 16 d d NOUN eurjchem-108 69 17     SPACE eurjchem-108 69 18 o o NOUN eurjchem-108 69 19     SPACE eurjchem-108 69 20 4‐f 4‐f NOUN eurjchem-108 69 21     SPACE eurjchem-108 69 22 5 5 NUM eurjchem-108 69 23     SPACE eurjchem-108 69 24 88 88 NUM eurjchem-108 69 25 301‐303 301‐303 NUM eurjchem-108 69 26     SPACE eurjchem-108 69 27 e e NOUN eurjchem-108 69 28     SPACE eurjchem-108 69 29 o o NOUN eurjchem-108 69 30     SPACE eurjchem-108 69 31 2‐cl 2‐cl NOUN eurjchem-108 69 32     SPACE eurjchem-108 69 33 8 8 NUM eurjchem-108 69 34     SPACE eurjchem-108 69 35 91/(55 91/(55 NUM eurjchem-108 69 36 ) ) PUNCT eurjchem-108 70 1 [ [ X eurjchem-108 70 2 3 3 NUM eurjchem-108 70 3 ] ] SYM eurjchem-108 70 4 285/(282‐283 285/(282‐283 NUM eurjchem-108 70 5 ) ) PUNCT eurjchem-108 70 6     SPACE eurjchem-108 71 1 [ [ X eurjchem-108 71 2 3 3 NUM eurjchem-108 71 3 ] ] SYM eurjchem-108 71 4     SPACE eurjchem-108 71 5 f f NUM eurjchem-108 71 6     SPACE eurjchem-108 71 7 o o NOUN eurjchem-108 71 8     SPACE eurjchem-108 71 9 3‐cl 3‐cl NUM eurjchem-108 71 10     SPACE eurjchem-108 71 11 6 6 NUM eurjchem-108 71 12     SPACE eurjchem-108 71 13 93/(56 93/(56 NUM eurjchem-108 71 14 ) ) PUNCT eurjchem-108 71 15     SPACE eurjchem-108 72 1 [ [ X eurjchem-108 72 2 3 3 NUM eurjchem-108 72 3 ] ] SYM eurjchem-108 72 4     SPACE eurjchem-108 72 5 276‐278/(275‐276 276‐278/(275‐276 NUM eurjchem-108 72 6 ) ) PUNCT eurjchem-108 72 7     SPACE eurjchem-108 73 1 [ [ X eurjchem-108 73 2 3 3 NUM eurjchem-108 73 3 ] ] SYM eurjchem-108 73 4     SPACE eurjchem-108 73 5 g g NOUN eurjchem-108 73 6     SPACE eurjchem-108 73 7 o o NOUN eurjchem-108 73 8     SPACE eurjchem-108 73 9 3‐br 3‐br NUM eurjchem-108 73 10     SPACE eurjchem-108 73 11 6 6 NUM eurjchem-108 73 12     SPACE eurjchem-108 73 13 85/(41 85/(41 NUM eurjchem-108 73 14 ) ) PUNCT eurjchem-108 73 15     SPACE eurjchem-108 73 16 [ [ X eurjchem-108 73 17 3 3 X eurjchem-108 73 18 ] ] SYM eurjchem-108 73 19 275‐277/(274‐275 275‐277/(274‐275 NUM eurjchem-108 73 20 ) ) PUNCT eurjchem-108 73 21     SPACE eurjchem-108 74 1 [ [ X eurjchem-108 74 2 3 3 NUM eurjchem-108 74 3 ] ] SYM eurjchem-108 74 4     SPACE eurjchem-108 74 5 h h NOUN eurjchem-108 74 6     SPACE eurjchem-108 74 7 o o NOUN eurjchem-108 74 8     SPACE eurjchem-108 74 9 4‐br 4‐br NOUN eurjchem-108 74 10     SPACE eurjchem-108 74 11 6 6 NUM eurjchem-108 74 12     SPACE eurjchem-108 74 13 90/44 90/44 NUM eurjchem-108 74 14 330/(>300 330/(>300 NUM eurjchem-108 74 15 ) ) PUNCT eurjchem-108 74 16     SPACE eurjchem-108 75 1 [ [ X eurjchem-108 75 2 3 3 NUM eurjchem-108 75 3 ] ] SYM eurjchem-108 75 4     SPACE eurjchem-108 75 5 i i PRON eurjchem-108 75 6     SPACE eurjchem-108 75 7 o o NOUN eurjchem-108 75 8     SPACE eurjchem-108 75 9 4‐no2 4‐no2 NOUN eurjchem-108 75 10     SPACE eurjchem-108 75 11 11 11 NUM eurjchem-108 75 12     SPACE eurjchem-108 75 13 80 80 NUM eurjchem-108 75 14 , , PUNCT eurjchem-108 75 15     SPACE eurjchem-108 75 16 78 78 NUM eurjchem-108 75 17 , , PUNCT eurjchem-108 75 18     SPACE eurjchem-108 75 19 75 75 NUM eurjchem-108 75 20     SPACE eurjchem-108 75 21 ( ( PUNCT eurjchem-108 75 22 3 3 NUM eurjchem-108 75 23     SPACE eurjchem-108 75 24 runs run NOUN eurjchem-108 75 25 ) ) PUNCT eurjchem-108 75 26 303‐305 303‐305 PROPN eurjchem-108 75 27     SPACE eurjchem-108 75 28 j j PROPN eurjchem-108 75 29     SPACE eurjchem-108 75 30 s s PROPN eurjchem-108 75 31     SPACE eurjchem-108 75 32 h h NOUN eurjchem-108 75 33     SPACE eurjchem-108 75 34 6 6 NUM eurjchem-108 75 35     SPACE eurjchem-108 75 36 85/(58 85/(58 NUM eurjchem-108 75 37 ) ) PUNCT eurjchem-108 76 1 [ [ X eurjchem-108 76 2 22 22 NUM eurjchem-108 76 3 ] ] SYM eurjchem-108 76 4 279‐281/(291‐293 279‐281/(291‐293 NUM eurjchem-108 76 5 ) ) PUNCT eurjchem-108 76 6     SPACE eurjchem-108 77 1 [ [ X eurjchem-108 77 2 22 22 NUM eurjchem-108 77 3 ] ] SYM eurjchem-108 77 4     SPACE eurjchem-108 77 5 k k X eurjchem-108 77 6     SPACE eurjchem-108 77 7 s s PART eurjchem-108 77 8     SPACE eurjchem-108 77 9 4‐ch3 4‐ch3 ADJ eurjchem-108 77 10     SPACE eurjchem-108 77 11 4 4 NUM eurjchem-108 77 12     SPACE eurjchem-108 77 13 81/(49 81/(49 NUM eurjchem-108 77 14 ) ) PUNCT eurjchem-108 78 1 [ [ X eurjchem-108 78 2 22 22 NUM eurjchem-108 78 3 ] ] SYM eurjchem-108 78 4 298‐300/(293‐296 298‐300/(293‐296 NUM eurjchem-108 78 5 ) ) PUNCT eurjchem-108 78 6     SPACE eurjchem-108 79 1 [ [ X eurjchem-108 79 2 22 22 NUM eurjchem-108 79 3 ] ] PUNCT eurjchem-108 79 4     SPACE eurjchem-108 79 5 l l NOUN eurjchem-108 79 6     SPACE eurjchem-108 79 7 s s PART eurjchem-108 79 8     SPACE eurjchem-108 79 9 3,4‐(och3)2 3,4‐(och3)2 NUM eurjchem-108 79 10     SPACE eurjchem-108 79 11 11 11 NUM eurjchem-108 79 12     SPACE eurjchem-108 79 13 76 76 NUM eurjchem-108 79 14 230‐232 230‐232 NUM eurjchem-108 79 15     SPACE eurjchem-108 79 16 m m VERB eurjchem-108 79 17     SPACE eurjchem-108 79 18 s s PART eurjchem-108 79 19     SPACE eurjchem-108 79 20 3‐cl 3‐cl NUM eurjchem-108 79 21     SPACE eurjchem-108 79 22 8 8 NUM eurjchem-108 79 23     SPACE eurjchem-108 79 24 86 86 NUM eurjchem-108 79 25 262‐264 262‐264 NUM eurjchem-108 79 26     SPACE eurjchem-108 79 27 n n CCONJ eurjchem-108 79 28     SPACE eurjchem-108 79 29 s s PROPN eurjchem-108 79 30     SPACE eurjchem-108 79 31 3‐br 3‐br NUM eurjchem-108 79 32     SPACE eurjchem-108 79 33 8 8 NUM eurjchem-108 79 34     SPACE eurjchem-108 79 35 87 87 NUM eurjchem-108 79 36 263‐264 263‐264 NUM eurjchem-108 79 37     SPACE eurjchem-108 79 38 o o NOUN eurjchem-108 79 39     SPACE eurjchem-108 79 40 s s NOUN eurjchem-108 79 41     SPACE eurjchem-108 79 42 4‐br 4‐br NOUN eurjchem-108 79 43     SPACE eurjchem-108 79 44 6 6 NUM eurjchem-108 79 45     SPACE eurjchem-108 79 46 89 89 NUM eurjchem-108 79 47 284‐286 284‐286 NUM eurjchem-108 79 48         SPACE eurjchem-108 79 49 4 4 NUM eurjchem-108 79 50 . . PUNCT eurjchem-108 79 51     SPACE eurjchem-108 79 52 conclusion conclusion NOUN eurjchem-108 79 53         SPACE eurjchem-108 79 54 in in ADP eurjchem-108 79 55     SPACE eurjchem-108 79 56 conclusion conclusion NOUN eurjchem-108 79 57 , , PUNCT eurjchem-108 79 58     SPACE eurjchem-108 79 59 the the DET eurjchem-108 79 60     SPACE eurjchem-108 79 61 present present ADJ eurjchem-108 79 62     SPACE eurjchem-108 79 63 procedure procedure NOUN eurjchem-108 79 64     SPACE eurjchem-108 79 65 provides provide VERB eurjchem-108 79 66     SPACE eurjchem-108 79 67 an an DET eurjchem-108 79 68     SPACE eurjchem-108 79 69 efficient efficient ADJ eurjchem-108 79 70     SPACE eurjchem-108 79 71 and and CCONJ eurjchem-108 79 72     SPACE eurjchem-108 79 73 improved improve VERB eurjchem-108 79 74     SPACE eurjchem-108 79 75 modification modification NOUN eurjchem-108 79 76     SPACE eurjchem-108 79 77 of of ADP eurjchem-108 79 78     SPACE eurjchem-108 79 79 the the DET eurjchem-108 79 80     SPACE eurjchem-108 79 81 biginelli biginelli NOUN eurjchem-108 79 82     SPACE eurjchem-108 79 83 reaction reaction NOUN eurjchem-108 79 84     SPACE eurjchem-108 79 85 for for ADP eurjchem-108 79 86     SPACE eurjchem-108 79 87 preparation preparation NOUN eurjchem-108 79 88     SPACE eurjchem-108 79 89 of of ADP eurjchem-108 79 90     SPACE eurjchem-108 79 91 octahydroquinazolinone octahydroquinazolinone NOUN eurjchem-108 79 92 . . PUNCT eurjchem-108 79 93     SPACE eurjchem-108 79 94 this this DET eurjchem-108 79 95     SPACE eurjchem-108 79 96 procedure procedure NOUN eurjchem-108 79 97     SPACE eurjchem-108 79 98 is be AUX eurjchem-108 79 99     SPACE eurjchem-108 79 100 associated associate VERB eurjchem-108 79 101     SPACE eurjchem-108 79 102 with with ADP eurjchem-108 79 103     SPACE eurjchem-108 79 104 some some DET eurjchem-108 79 105     SPACE eurjchem-108 79 106 advantages advantage NOUN eurjchem-108 79 107     SPACE eurjchem-108 79 108 such such ADJ eurjchem-108 79 109     SPACE eurjchem-108 79 110 as as ADP eurjchem-108 79 111     SPACE eurjchem-108 79 112 high high ADJ eurjchem-108 79 113     SPACE eurjchem-108 79 114 yields yield NOUN eurjchem-108 79 115 , , PUNCT eurjchem-108 79 116     SPACE eurjchem-108 79 117 ease ease NOUN eurjchem-108 79 118     SPACE eurjchem-108 79 119 of of ADP eurjchem-108 79 120     SPACE eurjchem-108 79 121 workup workup NOUN eurjchem-108 79 122     SPACE eurjchem-108 79 123 and and CCONJ eurjchem-108 79 124     SPACE eurjchem-108 79 125 reusability reusability NOUN eurjchem-108 79 126     SPACE eurjchem-108 79 127 of of ADP eurjchem-108 79 128     SPACE eurjchem-108 79 129 catalyst catalyst NOUN eurjchem-108 79 130 . . PUNCT eurjchem-108 79 131         SPACE eurjchem-108 80 1 acknowledgement acknowledgement NOUN eurjchem-108 80 2         SPACE eurjchem-108 80 3 we we PRON eurjchem-108 80 4     SPACE eurjchem-108 80 5 gratefully gratefully ADV eurjchem-108 80 6     SPACE eurjchem-108 80 7 acknowledge acknowledge VERB eurjchem-108 80 8     SPACE eurjchem-108 80 9 the the DET eurjchem-108 80 10     SPACE eurjchem-108 80 11 financial financial ADJ eurjchem-108 80 12     SPACE eurjchem-108 80 13 support support NOUN eurjchem-108 80 14     SPACE eurjchem-108 80 15 from from ADP eurjchem-108 80 16     SPACE eurjchem-108 80 17 the the DET eurjchem-108 80 18     SPACE eurjchem-108 80 19 research research NOUN eurjchem-108 80 20     SPACE eurjchem-108 80 21 council council NOUN eurjchem-108 80 22     SPACE eurjchem-108 80 23 of of ADP eurjchem-108 80 24     SPACE eurjchem-108 80 25 the the DET eurjchem-108 80 26     SPACE eurjchem-108 80 27 arak arak PROPN eurjchem-108 80 28     SPACE eurjchem-108 80 29 university university NOUN eurjchem-108 80 30 . . PUNCT eurjchem-108 80 31         SPACE eurjchem-108 81 1 references reference NOUN eurjchem-108 81 2         SPACE eurjchem-108 81 3 [ [ X eurjchem-108 81 4 1 1 NUM eurjchem-108 81 5 ] ] PUNCT eurjchem-108 81 6 . . PUNCT eurjchem-108 82 1 kappe kappe PROPN eurjchem-108 82 2 , , PUNCT eurjchem-108 82 3     SPACE eurjchem-108 82 4 c. c. PROPN eurjchem-108 82 5     SPACE eurjchem-108 82 6 o. o. PROPN eurjchem-108 82 7     SPACE eurjchem-108 82 8 eur eur PROPN eurjchem-108 82 9 . . PUNCT eurjchem-108 82 10     SPACE eurjchem-108 82 11 j. j. PROPN eurjchem-108 82 12     SPACE eurjchem-108 82 13 med med PROPN eurjchem-108 82 14 . . PUNCT eurjchem-108 82 15     SPACE eurjchem-108 82 16 chem chem NOUN eurjchem-108 82 17 . . PUNCT eurjchem-108 82 18     SPACE eurjchem-108 82 19 2000 2000 NUM eurjchem-108 82 20 , , PUNCT eurjchem-108 82 21     SPACE eurjchem-108 82 22 35 35 NUM eurjchem-108 82 23 , , PUNCT eurjchem-108 82 24     SPACE eurjchem-108 82 25 1043‐1052 1043‐1052 NUM eurjchem-108 82 26 . . PUNCT eurjchem-108 82 27       SPACE eurjchem-108 83 1 [ [ X eurjchem-108 83 2 2 2 NUM eurjchem-108 83 3 ] ] PUNCT eurjchem-108 83 4 . . PUNCT eurjchem-108 84 1 kung kung PROPN eurjchem-108 84 2 , , PUNCT eurjchem-108 84 3     SPACE eurjchem-108 84 4 p. p. NOUN eurjchem-108 84 5     SPACE eurjchem-108 84 6 ‐p ‐p PROPN eurjchem-108 84 7 . . PUNCT eurjchem-108 84 8 ; ; PUNCT eurjchem-108 84 9     SPACE eurjchem-108 84 10 casper casper NOUN eurjchem-108 84 11 , , PUNCT eurjchem-108 84 12     SPACE eurjchem-108 84 13 m. m. NOUN eurjchem-108 84 14     SPACE eurjchem-108 84 15 d. d. PROPN eurjchem-108 84 16 ; ; PUNCT eurjchem-108 84 17     SPACE eurjchem-108 84 18 cook cook VERB eurjchem-108 84 19 , , PUNCT eurjchem-108 84 20     SPACE eurjchem-108 84 21 k. k. PROPN eurjchem-108 84 22     SPACE eurjchem-108 84 23 l. l. PROPN eurjchem-108 84 24 ; ; PUNCT eurjchem-108 84 25     SPACE eurjchem-108 84 26 wilson‐lingardo wilson‐lingardo NOUN eurjchem-108 84 27 , , PUNCT eurjchem-108 84 28     SPACE eurjchem-108 84 29 l. l. PROPN eurjchem-108 84 30 ; ; PUNCT eurjchem-108 84 31     SPACE eurjchem-108 84 32 risen rise VERB eurjchem-108 84 33 , , PUNCT eurjchem-108 84 34     SPACE eurjchem-108 84 35 l. l. PROPN eurjchem-108 84 36     SPACE eurjchem-108 84 37 m. m. NOUN eurjchem-108 84 38 ; ; PUNCT eurjchem-108 84 39     SPACE eurjchem-108 84 40 vickers vicker NOUN eurjchem-108 84 41 , , PUNCT eurjchem-108 84 42     SPACE eurjchem-108 84 43 t. t. PROPN eurjchem-108 84 44     SPACE eurjchem-108 84 45 a. a. NOUN eurjchem-108 84 46 ; ; PUNCT eurjchem-108 84 47     SPACE eurjchem-108 84 48 ranken ranken VERB eurjchem-108 84 49 , , PUNCT eurjchem-108 84 50     SPACE eurjchem-108 84 51 r. r. PROPN eurjchem-108 84 52 ; ; PUNCT eurjchem-108 84 53     SPACE eurjchem-108 84 54 blyn blyn NOUN eurjchem-108 84 55 , , PUNCT eurjchem-108 84 56     SPACE eurjchem-108 84 57 l. l. PROPN eurjchem-108 84 58     SPACE eurjchem-108 84 59 b. b. PROPN eurjchem-108 84 60 ; ; PUNCT eurjchem-108 84 61     SPACE eurjchem-108 84 62 wyatt wyatt PROPN eurjchem-108 84 63 , , PUNCT eurjchem-108 84 64     SPACE eurjchem-108 84 65 j. j. PROPN eurjchem-108 84 66     SPACE eurjchem-108 84 67 r. r. PROPN eurjchem-108 84 68 ; ; PUNCT eurjchem-108 84 69     SPACE eurjchem-108 84 70 cook cook VERB eurjchem-108 84 71 , , PUNCT eurjchem-108 84 72     SPACE eurjchem-108 84 73 p. p. NOUN eurjchem-108 84 74     SPACE eurjchem-108 84 75 d. d. PROPN eurjchem-108 84 76 ; ; PUNCT eurjchem-108 84 77     SPACE eurjchem-108 84 78 ecker ecker NOUN eurjchem-108 84 79 , , PUNCT eurjchem-108 84 80     SPACE eurjchem-108 84 81 d. d. PROPN eurjchem-108 84 82     SPACE eurjchem-108 84 83 j. j. PROPN eurjchem-108 84 84       SPACE eurjchem-108 84 85 j. j. PROPN eurjchem-108 84 86     SPACE eurjchem-108 84 87 med med PROPN eurjchem-108 84 88 . . PUNCT eurjchem-108 84 89     SPACE eurjchem-108 84 90 chem chem NOUN eurjchem-108 84 91 . . PUNCT eurjchem-108 84 92     SPACE eurjchem-108 84 93 1999 1999 NUM eurjchem-108 84 94 , , PUNCT eurjchem-108 84 95     SPACE eurjchem-108 84 96 42 42 NUM eurjchem-108 84 97 , , PUNCT eurjchem-108 84 98     SPACE eurjchem-108 84 99 4705‐4713 4705‐4713 NUM eurjchem-108 84 100 . . PUNCT eurjchem-108 84 101       SPACE eurjchem-108 85 1 [ [ X eurjchem-108 85 2 3 3 NUM eurjchem-108 85 3 ] ] PUNCT eurjchem-108 85 4 . . PUNCT eurjchem-108 86 1 yarim yarim ADJ eurjchem-108 86 2 , , PUNCT eurjchem-108 86 3     SPACE eurjchem-108 86 4 m. m. NOUN eurjchem-108 86 5 ; ; PUNCT eurjchem-108 86 6     SPACE eurjchem-108 86 7 saraç saraç NOUN eurjchem-108 86 8 , , PUNCT eurjchem-108 86 9     SPACE eurjchem-108 86 10 s. s. PROPN eurjchem-108 86 11 ; ; PUNCT eurjchem-108 86 12     SPACE eurjchem-108 86 13 kiliç kiliç NOUN eurjchem-108 86 14 , , PUNCT eurjchem-108 86 15     SPACE eurjchem-108 86 16 f. f. PROPN eurjchem-108 86 17     SPACE eurjchem-108 86 18 s. s. PROPN eurjchem-108 86 19 ; ; PUNCT eurjchem-108 86 20     SPACE eurjchem-108 86 21 erol erol NOUN eurjchem-108 86 22 , , PUNCT eurjchem-108 86 23     SPACE eurjchem-108 86 24 k. k. PROPN eurjchem-108 86 25     SPACE eurjchem-108 86 26 il il PROPN eurjchem-108 86 27     SPACE eurjchem-108 86 28 farmaco farmaco PROPN eurjchem-108 86 29     SPACE eurjchem-108 86 30 2003 2003 NUM eurjchem-108 86 31 , , PUNCT eurjchem-108 86 32     SPACE eurjchem-108 86 33 58 58 NUM eurjchem-108 86 34 , , PUNCT eurjchem-108 86 35     SPACE eurjchem-108 86 36 17‐24 17‐24 NUM eurjchem-108 86 37 . . PUNCT eurjchem-108 86 38       SPACE eurjchem-108 87 1 [ [ X eurjchem-108 87 2 4 4 NUM eurjchem-108 87 3 ] ] PUNCT eurjchem-108 87 4 . . PUNCT eurjchem-108 88 1 v v NOUN eurjchem-108 88 2     SPACE eurjchem-108 88 3 alagarsamy alagarsamy NOUN eurjchem-108 88 4 , , PUNCT eurjchem-108 88 5     SPACE eurjchem-108 88 6 v. v. PROPN eurjchem-108 88 7 ; ; PUNCT eurjchem-108 88 8     SPACE eurjchem-108 88 9 pathak pathak PROPN eurjchem-108 88 10 , , PUNCT eurjchem-108 88 11     SPACE eurjchem-108 88 12 u. u. PROPN eurjchem-108 88 13     SPACE eurjchem-108 88 14 s. s. PROPN eurjchem-108 88 15 ; ; PUNCT eurjchem-108 88 16     SPACE eurjchem-108 88 17 sriram sriram PROPN eurjchem-108 88 18 , , PUNCT eurjchem-108 88 19     SPACE eurjchem-108 88 20 d. d. PROPN eurjchem-108 88 21 ; ; PUNCT eurjchem-108 88 22     SPACE eurjchem-108 88 23 pandeya pandeya NOUN eurjchem-108 88 24 , , PUNCT eurjchem-108 88 25     SPACE eurjchem-108 88 26 s. s. PROPN eurjchem-108 88 27     SPACE eurjchem-108 88 28 n. n. PROPN eurjchem-108 88 29 ; ; PUNCT eurjchem-108 88 30     SPACE eurjchem-108 88 31 clercq clercq NOUN eurjchem-108 88 32     SPACE eurjchem-108 88 33 e e PROPN eurjchem-108 88 34 , , PUNCT eurjchem-108 88 35     SPACE eurjchem-108 88 36 de de X eurjchem-108 88 37 . . NOUN eurjchem-108 88 38     SPACE eurjchem-108 88 39 ind ind PROPN eurjchem-108 88 40 . . PUNCT eurjchem-108 88 41     SPACE eurjchem-108 88 42 j. j. PROPN eurjchem-108 88 43     SPACE eurjchem-108 88 44 pharm pharm PROPN eurjchem-108 88 45 . . PUNCT eurjchem-108 88 46     SPACE eurjchem-108 89 1 sci sci PROPN eurjchem-108 89 2 . . PUNCT eurjchem-108 89 3     SPACE eurjchem-108 89 4 2000 2000 NUM eurjchem-108 89 5 , , PUNCT eurjchem-108 89 6     SPACE eurjchem-108 89 7 62 62 NUM eurjchem-108 89 8 , , PUNCT eurjchem-108 89 9     SPACE eurjchem-108 89 10 433‐437 433‐437 NUM eurjchem-108 89 11 . . PUNCT eurjchem-108 89 12       SPACE eurjchem-108 90 1 [ [ X eurjchem-108 90 2 5 5 NUM eurjchem-108 90 3 ] ] PUNCT eurjchem-108 90 4 . . PUNCT eurjchem-108 91 1 ladani ladani PROPN eurjchem-108 91 2 , , PUNCT eurjchem-108 91 3     SPACE eurjchem-108 91 4 n. n. PROPN eurjchem-108 91 5     SPACE eurjchem-108 91 6 k. k. PROPN eurjchem-108 91 7 ; ; PUNCT eurjchem-108 91 8     SPACE eurjchem-108 91 9 patel patel NOUN eurjchem-108 91 10 , , PUNCT eurjchem-108 91 11     SPACE eurjchem-108 91 12 m. m. NOUN eurjchem-108 91 13     SPACE eurjchem-108 91 14 p. p. NOUN eurjchem-108 91 15 ; ; PUNCT eurjchem-108 91 16     SPACE eurjchem-108 91 17 patel patel NOUN eurjchem-108 91 18 , , PUNCT eurjchem-108 91 19     SPACE eurjchem-108 91 20 r. r. PROPN eurjchem-108 91 21     SPACE eurjchem-108 91 22 g g PROPN eurjchem-108 91 23 , , PUNCT eurjchem-108 91 24     SPACE eurjchem-108 91 25 arkivoc arkivoc NOUN eurjchem-108 91 26     SPACE eurjchem-108 91 27 2009 2009 NUM eurjchem-108 91 28 , , PUNCT eurjchem-108 91 29     SPACE eurjchem-108 91 30 7 7 NUM eurjchem-108 91 31 , , PUNCT eurjchem-108 91 32     SPACE eurjchem-108 91 33 292‐302 292‐302 NOUN eurjchem-108 91 34 . . PUNCT eurjchem-108 91 35         SPACE eurjchem-108 92 1 [ [ X eurjchem-108 92 2 6 6 NUM eurjchem-108 92 3 ] ] PUNCT eurjchem-108 92 4 . . PUNCT eurjchem-108 93 1 vanden vanden PROPN eurjchem-108 93 2     SPACE eurjchem-108 93 3 eynde eynde NOUN eurjchem-108 93 4 , , PUNCT eurjchem-108 93 5     SPACE eurjchem-108 93 6 j. j. PROPN eurjchem-108 93 7     SPACE eurjchem-108 93 8 j. j. PROPN eurjchem-108 93 9 ; ; PUNCT eurjchem-108 93 10     SPACE eurjchem-108 93 11 godin godin NOUN eurjchem-108 93 12 , , PUNCT eurjchem-108 93 13     SPACE eurjchem-108 93 14 j. j. PROPN eurjchem-108 93 15 ; ; PUNCT eurjchem-108 93 16     SPACE eurjchem-108 93 17 mayence mayence NOUN eurjchem-108 93 18 , , PUNCT eurjchem-108 93 19     SPACE eurjchem-108 93 20 a. a. NOUN eurjchem-108 93 21 ; ; PUNCT eurjchem-108 93 22     SPACE eurjchem-108 93 23 maquestiau maquestiau PROPN eurjchem-108 93 24 , , PUNCT eurjchem-108 93 25     SPACE eurjchem-108 93 26 a. a. NOUN eurjchem-108 93 27 ; ; PUNCT eurjchem-108 93 28     SPACE eurjchem-108 93 29 anders ander NOUN eurjchem-108 93 30 , , PUNCT eurjchem-108 93 31     SPACE eurjchem-108 93 32 e. e. PROPN eurjchem-108 93 33     SPACE eurjchem-108 93 34 synthesis synthesis NOUN eurjchem-108 93 35     SPACE eurjchem-108 93 36 1993 1993 NUM eurjchem-108 93 37 , , PUNCT eurjchem-108 93 38     SPACE eurjchem-108 93 39 9 9 NUM eurjchem-108 93 40 , , PUNCT eurjchem-108 93 41     SPACE eurjchem-108 93 42 867‐869 867‐869 NOUN eurjchem-108 93 43 . . PUNCT eurjchem-108 93 44       SPACE eurjchem-108 94 1 [ [ X eurjchem-108 94 2 7 7 NUM eurjchem-108 94 3 ] ] PUNCT eurjchem-108 94 4 . . PUNCT eurjchem-108 95 1 kempter kempter PROPN eurjchem-108 95 2 , , PUNCT eurjchem-108 95 3     SPACE eurjchem-108 95 4 g. g. PROPN eurjchem-108 95 5 ; ; PUNCT eurjchem-108 95 6     SPACE eurjchem-108 95 7 ehrlichmann ehrlichmann NOUN eurjchem-108 95 8 , , PUNCT eurjchem-108 95 9     SPACE eurjchem-108 95 10 w. w. NOUN eurjchem-108 95 11 ; ; PUNCT eurjchem-108 95 12     SPACE eurjchem-108 95 13 plesse plesse NOUN eurjchem-108 95 14 , , PUNCT eurjchem-108 95 15     SPACE eurjchem-108 95 16 m. m. NOUN eurjchem-108 95 17 ; ; PUNCT eurjchem-108 95 18     SPACE eurjchem-108 95 19 lehm lehm ADJ eurjchem-108 95 20 , , PUNCT eurjchem-108 95 21     SPACE eurjchem-108 95 22 h. h. PROPN eurjchem-108 95 23     SPACE eurjchem-108 95 24 ‐u ‐u PROPN eurjchem-108 95 25 . . PUNCT eurjchem-108 95 26     SPACE eurjchem-108 95 27 j. j. PROPN eurjchem-108 95 28     SPACE eurjchem-108 95 29 pract pract PROPN eurjchem-108 95 30 . . PUNCT eurjchem-108 95 31     SPACE eurjchem-108 95 32 chem chem NOUN eurjchem-108 95 33 . . PUNCT eurjchem-108 95 34     SPACE eurjchem-108 95 35 1982 1982 NUM eurjchem-108 95 36 , , PUNCT eurjchem-108 95 37     SPACE eurjchem-108 95 38 324 324 NUM eurjchem-108 95 39 , , PUNCT eurjchem-108 95 40     SPACE eurjchem-108 95 41 832‐840 832‐840 NUM eurjchem-108 95 42 . . PUNCT eurjchem-108 95 43       SPACE eurjchem-108 96 1 [ [ X eurjchem-108 96 2 8 8 NUM eurjchem-108 96 3 ] ] PUNCT eurjchem-108 96 4 . . PUNCT eurjchem-108 97 1 hassani hassani PROPN eurjchem-108 97 2 , , PUNCT eurjchem-108 97 3     SPACE eurjchem-108 97 4 z. z. PROPN eurjchem-108 97 5 ; ; PUNCT eurjchem-108 97 6     SPACE eurjchem-108 97 7 islami islami NOUN eurjchem-108 97 8 , , PUNCT eurjchem-108 97 9     SPACE eurjchem-108 97 10 m. m. NOUN eurjchem-108 97 11     SPACE eurjchem-108 97 12 r. r. PROPN eurjchem-108 97 13 ; ; PUNCT eurjchem-108 97 14     SPACE eurjchem-108 97 15 kalantari kalantari ADJ eurjchem-108 97 16 , , PUNCT eurjchem-108 97 17     SPACE eurjchem-108 97 18 m. m. NOUN eurjchem-108 97 19     SPACE eurjchem-108 97 20 bioorg bioorg PROPN eurjchem-108 97 21 . . PUNCT eurjchem-108 97 22     SPACE eurjchem-108 97 23 med med PROPN eurjchem-108 97 24 . . PUNCT eurjchem-108 97 25     SPACE eurjchem-108 97 26 chem chem NOUN eurjchem-108 97 27 . . PUNCT eurjchem-108 97 28     SPACE eurjchem-108 98 1 lett lett PROPN eurjchem-108 98 2 . . PUNCT eurjchem-108 98 3     SPACE eurjchem-108 99 1 2000 2000 NUM eurjchem-108 99 2 , , PUNCT eurjchem-108 99 3     SPACE eurjchem-108 99 4 16 16 NUM eurjchem-108 99 5 , , PUNCT eurjchem-108 99 6     SPACE eurjchem-108 99 7 4479‐4482 4479‐4482 NUM eurjchem-108 99 8 . . PUNCT eurjchem-108 99 9       SPACE eurjchem-108 100 1 [ [ X eurjchem-108 100 2 9 9 NUM eurjchem-108 100 3 ] ] PUNCT eurjchem-108 100 4 . . PUNCT eurjchem-108 101 1 mobinikhaledi mobinikhaledi PROPN eurjchem-108 101 2 , , PUNCT eurjchem-108 101 3     SPACE eurjchem-108 101 4 a. a. NOUN eurjchem-108 101 5 ; ; PUNCT eurjchem-108 101 6     SPACE eurjchem-108 101 7 foroughifar foroughifar ADV eurjchem-108 101 8 , , PUNCT eurjchem-108 101 9     SPACE eurjchem-108 101 10 n. n. NOUN eurjchem-108 101 11 ; ; PUNCT eurjchem-108 101 12     SPACE eurjchem-108 101 13 karimi karimi X eurjchem-108 101 14 , , PUNCT eurjchem-108 101 15     SPACE eurjchem-108 101 16 g. g. NOUN eurjchem-108 101 17     SPACE eurjchem-108 101 18 synth synth NOUN eurjchem-108 101 19 . . PUNCT eurjchem-108 101 20     SPACE eurjchem-108 101 21 react react VERB eurjchem-108 101 22 . . PUNCT eurjchem-108 101 23     SPACE eurjchem-108 102 1 inorg inorg PROPN eurjchem-108 102 2 . . PUNCT eurjchem-108 102 3     SPACE eurjchem-108 103 1 m. m. NOUN eurjchem-108 103 2     SPACE eurjchem-108 103 3 2007 2007 NUM eurjchem-108 103 4 , , PUNCT eurjchem-108 103 5     SPACE eurjchem-108 103 6 37 37 NUM eurjchem-108 103 7 , , PUNCT eurjchem-108 103 8     SPACE eurjchem-108 103 9 279‐282 279‐282 NUM eurjchem-108 103 10 . . PUNCT eurjchem-108 103 11       SPACE eurjchem-108 104 1 [ [ X eurjchem-108 104 2 10 10 NUM eurjchem-108 104 3 ] ] PUNCT eurjchem-108 104 4 . . PUNCT eurjchem-108 104 5 zendehdel zendehdel PROPN eurjchem-108 104 6 , , PUNCT eurjchem-108 104 7     SPACE eurjchem-108 104 8 m. m. NOUN eurjchem-108 104 9 ; ; PUNCT eurjchem-108 104 10     SPACE eurjchem-108 104 11 mobinikhaledi mobinikhaledi ADJ eurjchem-108 104 12 . . PUNCT eurjchem-108 104 13     SPACE eurjchem-108 104 14 a. a. NOUN eurjchem-108 104 15 ; ; PUNCT eurjchem-108 104 16     SPACE eurjchem-108 104 17 asgari asgari ADJ eurjchem-108 104 18 , , PUNCT eurjchem-108 104 19     SPACE eurjchem-108 104 20 a. a. NOUN eurjchem-108 104 21     SPACE eurjchem-108 104 22 j. j. PROPN eurjchem-108 104 23     SPACE eurjchem-108 104 24 incl incl NOUN eurjchem-108 104 25 . . PUNCT eurjchem-108 104 26     SPACE eurjchem-108 104 27 phenom phenom PROPN eurjchem-108 104 28 . . PUNCT eurjchem-108 104 29     SPACE eurjchem-108 104 30 macro macro NOUN eurjchem-108 104 31 . . PUNCT eurjchem-108 104 32     SPACE eurjchem-108 104 33 2008 2008 NUM eurjchem-108 104 34 , , PUNCT eurjchem-108 104 35     SPACE eurjchem-108 104 36 60 60 NUM eurjchem-108 104 37 , , PUNCT eurjchem-108 104 38     SPACE eurjchem-108 104 39 353‐357 353‐357 NOUN eurjchem-108 104 40 . . PUNCT eurjchem-108 104 41       SPACE eurjchem-108 105 1 [ [ X eurjchem-108 105 2 11 11 NUM eurjchem-108 105 3 ] ] PUNCT eurjchem-108 105 4 . . PUNCT eurjchem-108 106 1 liu liu PROPN eurjchem-108 106 2 , , PUNCT eurjchem-108 106 3     SPACE eurjchem-108 106 4 c. c. NOUN eurjchem-108 106 5     SPACE eurjchem-108 106 6 ‐j ‐j NOUN eurjchem-108 106 7 . . PUNCT eurjchem-108 106 8 ; ; PUNCT eurjchem-108 106 9     SPACE eurjchem-108 106 10 wang wang PROPN eurjchem-108 106 11 , , PUNCT eurjchem-108 106 12     SPACE eurjchem-108 106 13 j. j. PROPN eurjchem-108 106 14     SPACE eurjchem-108 106 15 ‐d ‐d PROPN eurjchem-108 106 16 . . PUNCT eurjchem-108 106 17     SPACE eurjchem-108 106 18 molecules molecule NOUN eurjchem-108 106 19     SPACE eurjchem-108 106 20 2009 2009 NUM eurjchem-108 106 21 , , PUNCT eurjchem-108 106 22     SPACE eurjchem-108 106 23 14 14 NUM eurjchem-108 106 24 , , PUNCT eurjchem-108 106 25     SPACE eurjchem-108 106 26 763‐770 763‐770 NUM eurjchem-108 106 27 . . PUNCT eurjchem-108 106 28       SPACE eurjchem-108 107 1 [ [ X eurjchem-108 107 2 12 12 NUM eurjchem-108 107 3 ] ] PUNCT eurjchem-108 107 4 . . PUNCT eurjchem-108 108 1 dondoni dondoni NOUN eurjchem-108 108 2 , , PUNCT eurjchem-108 108 3     SPACE eurjchem-108 108 4 a. a. NOUN eurjchem-108 108 5 ; ; PUNCT eurjchem-108 108 6     SPACE eurjchem-108 108 7 massi massi PROPN eurjchem-108 108 8 , , PUNCT eurjchem-108 108 9     SPACE eurjchem-108 108 10 a. a. NOUN eurjchem-108 108 11 ; ; PUNCT eurjchem-108 108 12     SPACE eurjchem-108 108 13 minghini minghini NOUN eurjchem-108 108 14 , , PUNCT eurjchem-108 108 15     SPACE eurjchem-108 108 16 e. e. PROPN eurjchem-108 108 17 ; ; PUNCT eurjchem-108 108 18     SPACE eurjchem-108 108 19 sabbatini sabbatini PROPN eurjchem-108 108 20 , , PUNCT eurjchem-108 108 21     SPACE eurjchem-108 108 22 s. s. PROPN eurjchem-108 108 23 ; ; PUNCT eurjchem-108 108 24     SPACE eurjchem-108 108 25 bertolasi bertolasi NOUN eurjchem-108 108 26 , , PUNCT eurjchem-108 108 27     SPACE eurjchem-108 108 28 v. v. ADP eurjchem-108 108 29     SPACE eurjchem-108 108 30 j. j. PROPN eurjchem-108 108 31     SPACE eurjchem-108 108 32 org org PROPN eurjchem-108 108 33 . . PUNCT eurjchem-108 108 34     SPACE eurjchem-108 108 35 chem chem NOUN eurjchem-108 108 36 . . PUNCT eurjchem-108 108 37     SPACE eurjchem-108 108 38 2003 2003 NUM eurjchem-108 108 39 , , PUNCT eurjchem-108 108 40     SPACE eurjchem-108 108 41 68 68 NUM eurjchem-108 108 42 , , PUNCT eurjchem-108 108 43     SPACE eurjchem-108 108 44 6172‐6183 6172‐6183 NUM eurjchem-108 108 45 . . PUNCT eurjchem-108 108 46       SPACE eurjchem-108 109 1 [ [ X eurjchem-108 109 2 13 13 NUM eurjchem-108 109 3 ] ] PUNCT eurjchem-108 109 4 . . PUNCT eurjchem-108 110 1 tajbakhsh tajbakhsh PROPN eurjchem-108 110 2 , , PUNCT eurjchem-108 110 3     SPACE eurjchem-108 110 4 m. m. NOUN eurjchem-108 110 5 ; ; PUNCT eurjchem-108 110 6     SPACE eurjchem-108 110 7 mohajerani mohajerani NOUN eurjchem-108 110 8 , , PUNCT eurjchem-108 110 9     SPACE eurjchem-108 110 10 b. b. PROPN eurjchem-108 110 11 ; ; PUNCT eurjchem-108 110 12     SPACE eurjchem-108 110 13 heravi heravi NOUN eurjchem-108 110 14 , , PUNCT eurjchem-108 110 15     SPACE eurjchem-108 110 16 m. m. NOUN eurjchem-108 110 17     SPACE eurjchem-108 110 18 m. m. NOUN eurjchem-108 110 19 ; ; PUNCT eurjchem-108 110 20     SPACE eurjchem-108 110 21 ahmadi ahmadi PROPN eurjchem-108 110 22 , , PUNCT eurjchem-108 110 23     SPACE eurjchem-108 110 24 a. a. NOUN eurjchem-108 110 25     SPACE eurjchem-108 110 26 n. n. PROPN eurjchem-108 110 27     SPACE eurjchem-108 110 28 j. j. PROPN eurjchem-108 110 29     SPACE eurjchem-108 110 30 mol mol PROPN eurjchem-108 110 31 . . PROPN eurjchem-108 110 32     SPACE eurjchem-108 110 33 catal catal NOUN eurjchem-108 110 34 . . PUNCT eurjchem-108 110 35     SPACE eurjchem-108 111 1 a a DET eurjchem-108 111 2     SPACE eurjchem-108 111 3 2005 2005 NUM eurjchem-108 111 4 , , PUNCT eurjchem-108 111 5     SPACE eurjchem-108 111 6 236 236 NUM eurjchem-108 111 7 , , PUNCT eurjchem-108 111 8     SPACE eurjchem-108 111 9 216‐219 216‐219 PROPN eurjchem-108 111 10 . . PUNCT eurjchem-108 111 11       SPACE eurjchem-108 112 1 [ [ X eurjchem-108 112 2 14 14 NUM eurjchem-108 112 3 ] ] PUNCT eurjchem-108 112 4 . . PUNCT eurjchem-108 113 1 zolfigol zolfigol NOUN eurjchem-108 113 2 , , PUNCT eurjchem-108 113 3     SPACE eurjchem-108 113 4 m. m. NOUN eurjchem-108 113 5     SPACE eurjchem-108 113 6 a. a. NOUN eurjchem-108 113 7     SPACE eurjchem-108 113 8 tetrahedron tetrahedron NOUN eurjchem-108 113 9     SPACE eurjchem-108 113 10 2001 2001 NUM eurjchem-108 113 11 , , PUNCT eurjchem-108 113 12     SPACE eurjchem-108 113 13 57 57 NUM eurjchem-108 113 14 , , PUNCT eurjchem-108 113 15     SPACE eurjchem-108 113 16 9509‐9511 9509‐9511 NOUN eurjchem-108 113 17 . . PUNCT eurjchem-108 113 18       SPACE eurjchem-108 114 1 [ [ X eurjchem-108 114 2 15 15 NUM eurjchem-108 114 3 ] ] PUNCT eurjchem-108 114 4 . . PUNCT eurjchem-108 115 1 habibi habibi PROPN eurjchem-108 115 2 , , PUNCT eurjchem-108 115 3     SPACE eurjchem-108 115 4 d. d. PROPN eurjchem-108 115 5 ; ; PUNCT eurjchem-108 115 6     SPACE eurjchem-108 115 7 zolfigol zolfigol NOUN eurjchem-108 115 8 , , PUNCT eurjchem-108 115 9     SPACE eurjchem-108 115 10 m. m. NOUN eurjchem-108 115 11     SPACE eurjchem-108 115 12 a. a. NOUN eurjchem-108 115 13 ; ; PUNCT eurjchem-108 115 14     SPACE eurjchem-108 115 15 shiri shiri PROPN eurjchem-108 115 16 , , PUNCT eurjchem-108 115 17     SPACE eurjchem-108 115 18 m. m. NOUN eurjchem-108 115 19 ; ; PUNCT eurjchem-108 115 20     SPACE eurjchem-108 115 21 sedaghat sedaghat NOUN eurjchem-108 115 22 , , PUNCT eurjchem-108 115 23     SPACE eurjchem-108 115 24 a. a. NOUN eurjchem-108 115 25     SPACE eurjchem-108 115 26 s. s. PROPN eurjchem-108 115 27     SPACE eurjchem-108 115 28 afr afr PROPN eurjchem-108 115 29 . . PUNCT eurjchem-108 115 30     SPACE eurjchem-108 115 31 j. j. PROPN eurjchem-108 115 32     SPACE eurjchem-108 115 33 chem chem NOUN eurjchem-108 115 34 . . PUNCT eurjchem-108 115 35     SPACE eurjchem-108 115 36 2008 2008 NUM eurjchem-108 115 37 , , PUNCT eurjchem-108 115 38     SPACE eurjchem-108 115 39 61 61 NUM eurjchem-108 115 40 , , PUNCT eurjchem-108 115 41     SPACE eurjchem-108 115 42 93‐96 93‐96 NOUN eurjchem-108 115 43 . . PUNCT eurjchem-108 115 44       SPACE eurjchem-108 116 1 [ [ X eurjchem-108 116 2 16 16 NUM eurjchem-108 116 3 ] ] PUNCT eurjchem-108 116 4 . . PUNCT eurjchem-108 117 1 salehi salehi NOUN eurjchem-108 117 2 , , PUNCT eurjchem-108 117 3     SPACE eurjchem-108 117 4 p. p. NOUN eurjchem-108 117 5 ; ; PUNCT eurjchem-108 117 6     SPACE eurjchem-108 117 7 zolfigol zolfigol NOUN eurjchem-108 117 8 , , PUNCT eurjchem-108 117 9     SPACE eurjchem-108 117 10 m. m. NOUN eurjchem-108 117 11     SPACE eurjchem-108 117 12 a. a. NOUN eurjchem-108 117 13 ; ; PUNCT eurjchem-108 117 14     SPACE eurjchem-108 117 15 shirini shirini NOUN eurjchem-108 117 16 , , PUNCT eurjchem-108 117 17     SPACE eurjchem-108 117 18 f. f. PROPN eurjchem-108 117 19 ; ; PUNCT eurjchem-108 117 20     SPACE eurjchem-108 117 21 baghbanzadeh baghbanzadeh NOUN eurjchem-108 117 22 , , PUNCT eurjchem-108 117 23     SPACE eurjchem-108 117 24 m. m. NOUN eurjchem-108 117 25     SPACE eurjchem-108 117 26 curr curr PROPN eurjchem-108 117 27 . . PUNCT eurjchem-108 117 28     SPACE eurjchem-108 117 29 org org PROPN eurjchem-108 117 30 . . PUNCT eurjchem-108 117 31     SPACE eurjchem-108 117 32 chem chem NOUN eurjchem-108 117 33 . . PUNCT eurjchem-108 117 34     SPACE eurjchem-108 117 35 2006 2006 NUM eurjchem-108 117 36 , , PUNCT eurjchem-108 117 37     SPACE eurjchem-108 117 38 10 10 NUM eurjchem-108 117 39 , , PUNCT eurjchem-108 117 40     SPACE eurjchem-108 117 41 2171‐2189 2171‐2189 NUM eurjchem-108 117 42 . . PUNCT eurjchem-108 117 43       SPACE eurjchem-108 118 1 [ [ X eurjchem-108 118 2 17 17 NUM eurjchem-108 118 3 ] ] PUNCT eurjchem-108 118 4 . . PUNCT eurjchem-108 119 1 habibi habibi PROPN eurjchem-108 119 2 , , PUNCT eurjchem-108 119 3     SPACE eurjchem-108 119 4 d. d. PROPN eurjchem-108 119 5 ; ; PUNCT eurjchem-108 119 6     SPACE eurjchem-108 119 7 zolfigol zolfigol NOUN eurjchem-108 119 8 , , PUNCT eurjchem-108 119 9     SPACE eurjchem-108 119 10 m. m. NOUN eurjchem-108 119 11     SPACE eurjchem-108 119 12 a. a. NOUN eurjchem-108 119 13 ; ; PUNCT eurjchem-108 119 14     SPACE eurjchem-108 119 15 shirini shirini NOUN eurjchem-108 119 16 , , PUNCT eurjchem-108 119 17     SPACE eurjchem-108 119 18 f. f. PROPN eurjchem-108 119 19 ; ; PUNCT eurjchem-108 119 20     SPACE eurjchem-108 119 21 safaiee safaiee NOUN eurjchem-108 119 22 , , PUNCT eurjchem-108 119 23     SPACE eurjchem-108 119 24 m. m. NOUN eurjchem-108 119 25 ; ; PUNCT eurjchem-108 119 26     SPACE eurjchem-108 119 27 abedini abedini NOUN eurjchem-108 119 28 , , PUNCT eurjchem-108 119 29     SPACE eurjchem-108 119 30 m. m. NOUN eurjchem-108 119 31 ; ; PUNCT eurjchem-108 119 32     SPACE eurjchem-108 119 33 rahmani rahmani VERB eurjchem-108 119 34 , , PUNCT eurjchem-108 119 35     SPACE eurjchem-108 119 36 p. p. NOUN eurjchem-108 119 37     SPACE eurjchem-108 119 38 s. s. PROPN eurjchem-108 119 39     SPACE eurjchem-108 119 40 afr afr PROPN eurjchem-108 119 41 . . PUNCT eurjchem-108 119 42     SPACE eurjchem-108 120 1 j. j. PROPN eurjchem-108 120 2     SPACE eurjchem-108 120 3 chem chem NOUN eurjchem-108 120 4 . . PUNCT eurjchem-108 120 5     SPACE eurjchem-108 121 1 2007 2007 NUM eurjchem-108 121 2 , , PUNCT eurjchem-108 121 3     SPACE eurjchem-108 121 4 60 60 NUM eurjchem-108 121 5 , , PUNCT eurjchem-108 121 6     SPACE eurjchem-108 121 7 17‐19 17‐19 NUM eurjchem-108 121 8 . . PUNCT eurjchem-108 121 9       SPACE eurjchem-108 122 1 [ [ X eurjchem-108 122 2 18 18 NUM eurjchem-108 122 3 ] ] PUNCT eurjchem-108 122 4 . . PUNCT eurjchem-108 123 1 bamoniri bamoniri NOUN eurjchem-108 123 2 , , PUNCT eurjchem-108 123 3     SPACE eurjchem-108 123 4 a. a. NOUN eurjchem-108 123 5 ; ; PUNCT eurjchem-108 123 6     SPACE eurjchem-108 123 7 zolfigoi zolfigoi NOUN eurjchem-108 123 8 , , PUNCT eurjchem-108 123 9     SPACE eurjchem-108 123 10 m. m. NOUN eurjchem-108 123 11     SPACE eurjchem-108 123 12 a. a. NOUN eurjchem-108 123 13 ; ; PUNCT eurjchem-108 123 14     SPACE eurjchem-108 123 15 mohammadpoor‐baltork mohammadpoor‐baltork PROPN eurjchem-108 123 16 , , PUNCT eurjchem-108 123 17     SPACE eurjchem-108 123 18 i. i. NOUN eurjchem-108 123 19 ; ; PUNCT eurjchem-108 123 20     SPACE eurjchem-108 123 21 mirjalili mirjalili NOUN eurjchem-108 123 22 , , PUNCT eurjchem-108 123 23     SPACE eurjchem-108 123 24 b. b. PROPN eurjchem-108 123 25     SPACE eurjchem-108 123 26 f. f. PROPN eurjchem-108 123 27     SPACE eurjchem-108 123 28 j. j. PROPN eurjchem-108 123 29     SPACE eurjchem-108 123 30 ir ir PROPN eurjchem-108 123 31 . . PUNCT eurjchem-108 123 32     SPACE eurjchem-108 123 33 chem chem NOUN eurjchem-108 123 34 . . PUNCT eurjchem-108 123 35     SPACE eurjchem-108 123 36 soc soc PROPN eurjchem-108 123 37 . . PUNCT eurjchem-108 123 38     SPACE eurjchem-108 123 39 2006 2006 NUM eurjchem-108 123 40 , , PUNCT eurjchem-108 123 41     SPACE eurjchem-108 123 42 3 3 NUM eurjchem-108 123 43 , , PUNCT eurjchem-108 123 44     SPACE eurjchem-108 123 45 85‐88 85‐88 NOUN eurjchem-108 123 46 . . PUNCT eurjchem-108 123 47       SPACE eurjchem-108 124 1 [ [ X eurjchem-108 124 2 19 19 NUM eurjchem-108 124 3 ] ] PUNCT eurjchem-108 124 4 . . PUNCT eurjchem-108 125 1 foroughifar foroughifar ADV eurjchem-108 125 2 , , PUNCT eurjchem-108 125 3     SPACE eurjchem-108 125 4 n. n. NOUN eurjchem-108 125 5 ; ; PUNCT eurjchem-108 125 6     SPACE eurjchem-108 125 7 mobinikhaledi mobinikhaledi ADJ eurjchem-108 125 8 , , PUNCT eurjchem-108 125 9     SPACE eurjchem-108 125 10 a. a. NOUN eurjchem-108 125 11 ; ; PUNCT eurjchem-108 125 12     SPACE eurjchem-108 125 13 fathinajad fathinajad NOUN eurjchem-108 125 14 , , PUNCT eurjchem-108 125 15     SPACE eurjchem-108 125 16 h. h. NOUN eurjchem-108 125 17     SPACE eurjchem-108 125 18 phosphorus phosphorus NOUN eurjchem-108 125 19 . . PUNCT eurjchem-108 125 20     SPACE eurjchem-108 126 1 sulfur sulfur NOUN eurjchem-108 126 2 . . PUNCT eurjchem-108 126 3     SPACE eurjchem-108 127 1 2003 2003 NUM eurjchem-108 127 2 , , PUNCT eurjchem-108 127 3     SPACE eurjchem-108 127 4 178 178 NUM eurjchem-108 127 5 , , PUNCT eurjchem-108 127 6     SPACE eurjchem-108 127 7 1241‐1246 1241‐1246 NUM eurjchem-108 127 8 . . PUNCT eurjchem-108 127 9       SPACE eurjchem-108 128 1 [ [ X eurjchem-108 128 2 20 20 NUM eurjchem-108 128 3 ] ] PUNCT eurjchem-108 128 4 . . PUNCT eurjchem-108 129 1 mobinikhaledi mobinikhaledi PROPN eurjchem-108 129 2 , , PUNCT eurjchem-108 129 3     SPACE eurjchem-108 129 4 a. a. NOUN eurjchem-108 129 5 ; ; PUNCT eurjchem-108 129 6     SPACE eurjchem-108 129 7 foroughifar foroughifar ADV eurjchem-108 129 8 , , PUNCT eurjchem-108 129 9     SPACE eurjchem-108 129 10 n. n. NOUN eurjchem-108 129 11 ; ; PUNCT eurjchem-108 129 12     SPACE eurjchem-108 129 13 fathinajad fathinajad NOUN eurjchem-108 129 14 , , PUNCT eurjchem-108 129 15     SPACE eurjchem-108 129 16 h. h. NOUN eurjchem-108 129 17     SPACE eurjchem-108 129 18 phosphorus phosphorus NOUN eurjchem-108 129 19 . . PUNCT eurjchem-108 129 20     SPACE eurjchem-108 129 21 sulfur sulfur NOUN eurjchem-108 129 22 . . PUNCT eurjchem-108 129 23     SPACE eurjchem-108 129 24 2004 2004 NUM eurjchem-108 129 25 , , PUNCT eurjchem-108 129 26     SPACE eurjchem-108 129 27 179 179 NUM eurjchem-108 129 28 , , PUNCT eurjchem-108 129 29     SPACE eurjchem-108 129 30 2259‐2263 2259‐2263 NUM eurjchem-108 129 31 . . PUNCT eurjchem-108 129 32       SPACE eurjchem-108 130 1 [ [ X eurjchem-108 130 2 21 21 NUM eurjchem-108 130 3 ] ] PUNCT eurjchem-108 130 4 . . PUNCT eurjchem-108 131 1 foroughifar foroughifar ADV eurjchem-108 131 2 , , PUNCT eurjchem-108 131 3     SPACE eurjchem-108 131 4 n. n. NOUN eurjchem-108 131 5 ; ; PUNCT eurjchem-108 131 6     SPACE eurjchem-108 131 7 mobinikhaledi mobinikhaledi ADJ eurjchem-108 131 8 , , PUNCT eurjchem-108 131 9     SPACE eurjchem-108 131 10 a. a. NOUN eurjchem-108 131 11 ; ; PUNCT eurjchem-108 131 12     SPACE eurjchem-108 131 13 shariatzadeh shariatzadeh NOUN eurjchem-108 131 14 , , PUNCT eurjchem-108 131 15     SPACE eurjchem-108 131 16 s. s. PROPN eurjchem-108 131 17     SPACE eurjchem-108 131 18 m. m. NOUN eurjchem-108 131 19 ; ; PUNCT eurjchem-108 131 20     SPACE eurjchem-108 131 21 masoudnia masoudnia NOUN eurjchem-108 131 22 , , PUNCT eurjchem-108 131 23     SPACE eurjchem-108 131 24 m. m. NOUN eurjchem-108 131 25     SPACE eurjchem-108 131 26 asian asian PROPN eurjchem-108 131 27     SPACE eurjchem-108 131 28 j. j. PROPN eurjchem-108 131 29     SPACE eurjchem-108 131 30 chem chem NOUN eurjchem-108 131 31 . . PUNCT eurjchem-108 131 32     SPACE eurjchem-108 132 1 2002 2002 NUM eurjchem-108 132 2 , , PUNCT eurjchem-108 132 3     SPACE eurjchem-108 132 4 14 14 NUM eurjchem-108 132 5 , , PUNCT eurjchem-108 132 6     SPACE eurjchem-108 132 7 782‐790 782‐790 NUM eurjchem-108 132 8 . . PUNCT eurjchem-108 132 9       SPACE eurjchem-108 133 1 [ [ X eurjchem-108 133 2 22 22 NUM eurjchem-108 133 3 ] ] PUNCT eurjchem-108 133 4 . . PUNCT eurjchem-108 134 1 shaabani shaabani PROPN eurjchem-108 134 2 , , PUNCT eurjchem-108 134 3     SPACE eurjchem-108 134 4 a. a. NOUN eurjchem-108 134 5 ; ; PUNCT eurjchem-108 134 6     SPACE eurjchem-108 134 7 sarvary sarvary ADJ eurjchem-108 134 8 , , PUNCT eurjchem-108 134 9     SPACE eurjchem-108 134 10 a. a. NOUN eurjchem-108 134 11 ; ; PUNCT eurjchem-108 134 12     SPACE eurjchem-108 134 13 rahmati rahmati NOUN eurjchem-108 134 14 , , PUNCT eurjchem-108 134 15     SPACE eurjchem-108 134 16 a. a. NOUN eurjchem-108 134 17 ; ; PUNCT eurjchem-108 134 18     SPACE eurjchem-108 134 19 rezayan rezayan NOUN eurjchem-108 134 20 , , PUNCT eurjchem-108 134 21     SPACE eurjchem-108 134 22 a. a. NOUN eurjchem-108 134 23     SPACE eurjchem-108 134 24 h. h. PROPN eurjchem-108 134 25     SPACE eurjchem-108 134 26 lett lett PROPN eurjchem-108 134 27 . . PUNCT eurjchem-108 134 28     SPACE eurjchem-108 134 29 org org PROPN eurjchem-108 134 30 . . PUNCT eurjchem-108 134 31     SPACE eurjchem-108 134 32 chem chem NOUN eurjchem-108 134 33 . . PUNCT eurjchem-108 134 34     SPACE eurjchem-108 134 35 2007 2007 NUM eurjchem-108 134 36 , , PUNCT eurjchem-108 134 37     SPACE eurjchem-108 134 38 4 4 NUM eurjchem-108 134 39 , , PUNCT eurjchem-108 134 40     SPACE eurjchem-108 134 41 68‐71 68‐71 NOUN eurjchem-108 134 42 . . PUNCT eurjchem-108 134 43       SPACE eurjchem-108 135 1 [ [ X eurjchem-108 135 2 23 23 NUM eurjchem-108 135 3 ] ] PUNCT eurjchem-108 135 4 . . PUNCT eurjchem-108 136 1 sabitha sabitha PROPN eurjchem-108 136 2 , , PUNCT eurjchem-108 136 3     SPACE eurjchem-108 136 4 g. g. NOUN eurjchem-108 136 5 ; ; PUNCT eurjchem-108 136 6     SPACE eurjchem-108 136 7 reddy reddy NOUN eurjchem-108 136 8 , , PUNCT eurjchem-108 136 9     SPACE eurjchem-108 136 10 k. k. PROPN eurjchem-108 136 11     SPACE eurjchem-108 136 12 b. b. PROPN eurjchem-108 136 13 ; ; PUNCT eurjchem-108 136 14     SPACE eurjchem-108 136 15 yadav yadav PROPN eurjchem-108 136 16 , , PUNCT eurjchem-108 136 17     SPACE eurjchem-108 136 18 j. j. PROPN eurjchem-108 136 19     SPACE eurjchem-108 136 20 s. s. PROPN eurjchem-108 136 21     SPACE eurjchem-108 136 22 tetrahedron tetrahedron NOUN eurjchem-108 136 23     SPACE eurjchem-108 136 24 let let VERB eurjchem-108 136 25 . . PUNCT eurjchem-108 136 26     SPACE eurjchem-108 136 27 2003 2003 NUM eurjchem-108 136 28 , , PUNCT eurjchem-108 136 29     SPACE eurjchem-108 136 30 44 44 NUM eurjchem-108 136 31 , , PUNCT eurjchem-108 136 32     SPACE eurjchem-108 136 33 6497‐ 6497‐ NUM eurjchem-108 136 34 6499 6499 NUM eurjchem-108 136 35 . . PUNCT eurjchem-108 136 36     SPACE