id	sid	tid	token	lemma	pos
eurjchem-1080	1	1	untitled	untitle	VERB
eurjchem-1080	1	2	european	european	PROPN
eurjchem-1080	1	3	journal	journal	PROPN
eurjchem-1080	1	4	of	of	ADP
eurjchem-1080	1	5	chemistry	chemistry	NOUN
eurjchem-1080	1	6	5	5	NUM
eurjchem-1080	1	7	(	(	PUNCT
eurjchem-1080	1	8	3	3	NUM
eurjchem-1080	1	9	)	)	PUNCT
eurjchem-1080	1	10	(	(	PUNCT
eurjchem-1080	1	11	2014	2014	NUM
eurjchem-1080	1	12	)	)	PUNCT
eurjchem-1080	1	13	497‐502	497‐502	PROPN
eurjchem-1080	1	14	european	european	ADJ
eurjchem-1080	1	15	journal	journal	PROPN
eurjchem-1080	1	16	of	of	ADP
eurjchem-1080	1	17	chemistry	chemistry	NOUN
eurjchem-1080	1	18	issn	issn	PROPN
eurjchem-1080	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-1080	1	20	(	(	PUNCT
eurjchem-1080	1	21	print	print	NOUN
eurjchem-1080	1	22	)	)	PUNCT
eurjchem-1080	1	23	/	/	SYM
eurjchem-1080	1	24	issn	issn	PROPN
eurjchem-1080	1	25	2153‐2257	2153‐2257	NUM
eurjchem-1080	1	26	(	(	PUNCT
eurjchem-1080	1	27	online	online	ADJ
eurjchem-1080	1	28	)	)	PUNCT
eurjchem-1080	1	29			NOUN
eurjchem-1080	1	30	2014	2014	NUM
eurjchem-1080	2	1	eurjchem	eurjchem	PROPN
eurjchem-1080	2	2	publishing	publish	VERB
eurjchem-1080	2	3	‐	‐	NOUN
eurjchem-1080	2	4	printed	print	VERB
eurjchem-1080	2	5	in	in	ADP
eurjchem-1080	2	6	the	the	DET
eurjchem-1080	2	7	usa	usa	PROPN
eurjchem-1080	2	8	http://dx.doi.org/10.5155/eurjchem.5.3.497‐502.1080	http://dx.doi.org/10.5155/eurjchem.5.3.497‐502.1080	PROPN
eurjchem-1080	2	9	european	european	PROPN
eurjchem-1080	2	10	journal	journal	PROPN
eurjchem-1080	2	11	of	of	ADP
eurjchem-1080	2	12	chemistry	chemistry	PROPN
eurjchem-1080	2	13	journal	journal	PROPN
eurjchem-1080	2	14	homepage	homepage	NOUN
eurjchem-1080	2	15	:	:	PUNCT
eurjchem-1080	2	16	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1080	2	17	a	a	DET
eurjchem-1080	2	18	validated	validate	VERB
eurjchem-1080	2	19	stability	stability	NOUN
eurjchem-1080	2	20	indicating	indicate	VERB
eurjchem-1080	2	21	hplc	hplc	NOUN
eurjchem-1080	2	22	method	method	NOUN
eurjchem-1080	2	23	for	for	ADP
eurjchem-1080	2	24	determination	determination	NOUN
eurjchem-1080	2	25	of	of	ADP
eurjchem-1080	2	26	sitagliptin	sitagliptin	PROPN
eurjchem-1080	2	27	ola	ola	PROPN
eurjchem-1080	2	28	ahmed	ahmed	PROPN
eurjchem-1080	2	29	saleh	saleh	PROPN
eurjchem-1080	2	30	a	a	PROPN
eurjchem-1080	2	31	,	,	PUNCT
eurjchem-1080	2	32	aida	aida	PROPN
eurjchem-1080	2	33	abd	abd	PROPN
eurjchem-1080	2	34	el‐sattar	el‐sattar	PROPN
eurjchem-1080	2	35	el‐azzouny	el‐azzouny	PROPN
eurjchem-1080	2	36	a	a	PROPN
eurjchem-1080	2	37	,	,	PUNCT
eurjchem-1080	2	38	hassan	hassan	PROPN
eurjchem-1080	2	39	youssef	youssef	PROPN
eurjchem-1080	2	40	aboul‐enein	aboul‐enein	X
eurjchem-1080	2	41	a	a	PRON
eurjchem-1080	2	42	,	,	PUNCT
eurjchem-1080	2	43	*	*	PUNCT
eurjchem-1080	2	44	and	and	CCONJ
eurjchem-1080	2	45	amr	amr	PROPN
eurjchem-1080	2	46	mohamed	mohamed	PROPN
eurjchem-1080	2	47	badawey	badawey	PROPN
eurjchem-1080	3	1	b	b	PROPN
eurjchem-1080	3	2	a	a	DET
eurjchem-1080	3	3	medicinal	medicinal	ADJ
eurjchem-1080	3	4	and	and	CCONJ
eurjchem-1080	3	5	pharmaceutical	pharmaceutical	ADJ
eurjchem-1080	3	6	chemistry	chemistry	NOUN
eurjchem-1080	3	7	department	department	NOUN
eurjchem-1080	3	8	,	,	PUNCT
eurjchem-1080	3	9	pharmaceutical	pharmaceutical	NOUN
eurjchem-1080	3	10	and	and	CCONJ
eurjchem-1080	3	11	drug	drug	NOUN
eurjchem-1080	3	12	industries	industry	NOUN
eurjchem-1080	3	13	research	research	NOUN
eurjchem-1080	3	14	division	division	NOUN
eurjchem-1080	3	15	,	,	PUNCT
eurjchem-1080	3	16	national	national	ADJ
eurjchem-1080	3	17	research	research	NOUN
eurjchem-1080	3	18	centre	centre	NOUN
eurjchem-1080	3	19	,	,	PUNCT
eurjchem-1080	3	20	12311	12311	NUM
eurjchem-1080	3	21	dokki	dokki	NOUN
eurjchem-1080	3	22	,	,	PUNCT
eurjchem-1080	3	23	cairo	cairo	PROPN
eurjchem-1080	3	24	,	,	PUNCT
eurjchem-1080	3	25	egypt	egypt	PROPN
eurjchem-1080	3	26	b	b	PROPN
eurjchem-1080	3	27	pharmaceutical	pharmaceutical	ADJ
eurjchem-1080	3	28	chemistry	chemistry	NOUN
eurjchem-1080	3	29	department	department	NOUN
eurjchem-1080	3	30	,	,	PUNCT
eurjchem-1080	3	31	faculty	faculty	NOUN
eurjchem-1080	3	32	of	of	ADP
eurjchem-1080	3	33	pharmaceutical	pharmaceutical	ADJ
eurjchem-1080	3	34	sciences	science	NOUN
eurjchem-1080	3	35	and	and	CCONJ
eurjchem-1080	3	36	pharmaceutical	pharmaceutical	NOUN
eurjchem-1080	3	37	industries	industry	NOUN
eurjchem-1080	3	38	,	,	PUNCT
eurjchem-1080	3	39	future	future	ADJ
eurjchem-1080	3	40	university	university	NOUN
eurjchem-1080	3	41	,	,	PUNCT
eurjchem-1080	3	42	12311	12311	NUM
eurjchem-1080	3	43	,	,	PUNCT
eurjchem-1080	3	44	cairo	cairo	PROPN
eurjchem-1080	3	45	,	,	PUNCT
eurjchem-1080	3	46	egypt	egypt	PROPN
eurjchem-1080	3	47	*	*	PUNCT
eurjchem-1080	3	48	corresponding	correspond	VERB
eurjchem-1080	3	49	author	author	NOUN
eurjchem-1080	3	50	at	at	ADP
eurjchem-1080	3	51	:	:	PUNCT
eurjchem-1080	3	52	medicinal	medicinal	ADJ
eurjchem-1080	3	53	and	and	CCONJ
eurjchem-1080	3	54	pharmaceutical	pharmaceutical	ADJ
eurjchem-1080	3	55	chemistry	chemistry	NOUN
eurjchem-1080	3	56	department	department	NOUN
eurjchem-1080	3	57	,	,	PUNCT
eurjchem-1080	3	58	pharmaceutical	pharmaceutical	NOUN
eurjchem-1080	3	59	and	and	CCONJ
eurjchem-1080	3	60	drug	drug	NOUN
eurjchem-1080	3	61	industries	industry	NOUN
eurjchem-1080	3	62	research	research	NOUN
eurjchem-1080	3	63	division	division	NOUN
eurjchem-1080	3	64	,	,	PUNCT
eurjchem-1080	3	65	national	national	ADJ
eurjchem-1080	3	66	research	research	NOUN
eurjchem-1080	3	67	centre	centre	NOUN
eurjchem-1080	3	68	,	,	PUNCT
eurjchem-1080	3	69	12311	12311	NUM
eurjchem-1080	3	70	dokki	dokki	NOUN
eurjchem-1080	3	71	,	,	PUNCT
eurjchem-1080	3	72	cairo	cairo	PROPN
eurjchem-1080	3	73	,	,	PUNCT
eurjchem-1080	3	74	egypt	egypt	PROPN
eurjchem-1080	3	75	.	.	PUNCT
eurjchem-1080	4	1	tel	tel	PROPN
eurjchem-1080	4	2	.	.	PUNCT
eurjchem-1080	4	3	:	:	PUNCT
eurjchem-1080	5	1	+20.2.33335454	+20.2.33335454	PROPN
eurjchem-1080	5	2	.	.	PUNCT
eurjchem-1080	6	1	fax	fax	NOUN
eurjchem-1080	6	2	:	:	PUNCT
eurjchem-1080	6	3	+20.2.33370931	+20.2.33370931	ADJ
eurjchem-1080	6	4	.	.	PUNCT
eurjchem-1080	6	5	e‐mail	e‐mail	PUNCT
eurjchem-1080	7	1	address	address	NOUN
eurjchem-1080	7	2	:	:	PUNCT
eurjchem-1080	7	3	haboulenein@yahoo.com	haboulenein@yahoo.com	X
eurjchem-1080	7	4	(	(	PUNCT
eurjchem-1080	7	5	h.y	h.y	PROPN
eurjchem-1080	7	6	.	.	PROPN
eurjchem-1080	7	7	aboul‐enein	aboul‐enein	PROPN
eurjchem-1080	7	8	)	)	PUNCT
eurjchem-1080	7	9	.	.	PUNCT
eurjchem-1080	8	1	article	article	NOUN
eurjchem-1080	8	2	information	information	PROPN
eurjchem-1080	8	3	abstract	abstract	ADJ
eurjchem-1080	8	4	doi	doi	NOUN
eurjchem-1080	8	5	:	:	PUNCT
eurjchem-1080	8	6	10.5155	10.5155	NUM
eurjchem-1080	8	7	/	/	SYM
eurjchem-1080	8	8	eurjchem.5.3.497‐502.1080	eurjchem.5.3.497‐502.1080	PUNCT
eurjchem-1080	8	9	received	receive	VERB
eurjchem-1080	8	10	:	:	PUNCT
eurjchem-1080	8	11	22	22	NUM
eurjchem-1080	8	12	april	april	PROPN
eurjchem-1080	8	13	2014	2014	NUM
eurjchem-1080	8	14	received	receive	VERB
eurjchem-1080	8	15	in	in	ADP
eurjchem-1080	8	16	revised	revise	VERB
eurjchem-1080	8	17	form	form	NOUN
eurjchem-1080	8	18	:	:	PUNCT
eurjchem-1080	8	19	21	21	NUM
eurjchem-1080	8	20	may	may	PROPN
eurjchem-1080	8	21	2014	2014	NUM
eurjchem-1080	8	22	accepted	accept	VERB
eurjchem-1080	8	23	:	:	PUNCT
eurjchem-1080	8	24	21	21	NUM
eurjchem-1080	8	25	may	may	PROPN
eurjchem-1080	8	26	2014	2014	NUM
eurjchem-1080	8	27	online	online	NOUN
eurjchem-1080	8	28	:	:	PUNCT
eurjchem-1080	8	29	30	30	NUM
eurjchem-1080	8	30	september	september	PROPN
eurjchem-1080	8	31	2014	2014	NUM
eurjchem-1080	8	32	keywords	keyword	VERB
eurjchem-1080	8	33	a	a	DET
eurjchem-1080	8	34	comparative	comparative	ADJ
eurjchem-1080	8	35	and	and	CCONJ
eurjchem-1080	8	36	stability‐indicating	stability‐indicate	VERB
eurjchem-1080	8	37	reversed	reverse	VERB
eurjchem-1080	8	38	phase	phase	NOUN
eurjchem-1080	8	39	high	high	ADJ
eurjchem-1080	8	40	performance	performance	NOUN
eurjchem-1080	8	41	liquid	liquid	ADJ
eurjchem-1080	8	42	chromatographic	chromatographic	ADJ
eurjchem-1080	8	43	study	study	NOUN
eurjchem-1080	8	44	have	have	AUX
eurjchem-1080	8	45	been	be	AUX
eurjchem-1080	8	46	developed	develop	VERB
eurjchem-1080	8	47	and	and	CCONJ
eurjchem-1080	8	48	validated	validate	VERB
eurjchem-1080	8	49	for	for	ADP
eurjchem-1080	8	50	sitagliptin	sitagliptin	NOUN
eurjchem-1080	8	51	phosphate	phosphate	NOUN
eurjchem-1080	8	52	.	.	PUNCT
eurjchem-1080	9	1	the	the	DET
eurjchem-1080	9	2	liquid	liquid	ADJ
eurjchem-1080	9	3	chromatographic	chromatographic	ADJ
eurjchem-1080	9	4	determination	determination	NOUN
eurjchem-1080	9	5	was	be	AUX
eurjchem-1080	9	6	achieved	achieve	VERB
eurjchem-1080	9	7	isocratically	isocratically	ADV
eurjchem-1080	9	8	on	on	ADP
eurjchem-1080	9	9	poroshell	poroshell	PROPN
eurjchem-1080	9	10	120	120	NUM
eurjchem-1080	9	11	ec‐c18	ec‐c18	NOUN
eurjchem-1080	9	12	(	(	PUNCT
eurjchem-1080	9	13	100	100	NUM
eurjchem-1080	9	14	×	×	NOUN
eurjchem-1080	9	15	4.6	4.6	NUM
eurjchem-1080	9	16	mm	mm	NOUN
eurjchem-1080	9	17	,	,	PUNCT
eurjchem-1080	9	18	i.d	i.d	PROPN
eurjchem-1080	9	19	.	.	PROPN
eurjchem-1080	9	20	;	;	PUNCT
eurjchem-1080	9	21	particle	particle	NOUN
eurjchem-1080	9	22	size	size	NOUN
eurjchem-1080	9	23	,	,	PUNCT
eurjchem-1080	9	24	2.7	2.7	NUM
eurjchem-1080	9	25	µm	µm	NOUN
eurjchem-1080	9	26	)	)	PUNCT
eurjchem-1080	9	27	,	,	PUNCT
eurjchem-1080	9	28	pursuit	pursuit	VERB
eurjchem-1080	9	29	5pfp	5pfp	NUM
eurjchem-1080	9	30	(	(	PUNCT
eurjchem-1080	9	31	150	150	NUM
eurjchem-1080	9	32	×	×	NOUN
eurjchem-1080	9	33	4.6	4.6	NUM
eurjchem-1080	9	34	mm	mm	NOUN
eurjchem-1080	9	35	,	,	PUNCT
eurjchem-1080	9	36	i.d	i.d	PROPN
eurjchem-1080	9	37	.	.	PROPN
eurjchem-1080	9	38	;	;	PUNCT
eurjchem-1080	9	39	particle	particle	NOUN
eurjchem-1080	9	40	size	size	NOUN
eurjchem-1080	9	41	,	,	PUNCT
eurjchem-1080	9	42	5	5	NUM
eurjchem-1080	9	43	µm	µm	NOUN
eurjchem-1080	9	44	)	)	PUNCT
eurjchem-1080	9	45	and	and	CCONJ
eurjchem-1080	9	46	chromolith	chromolith	VERB
eurjchem-1080	9	47	performance	performance	NOUN
eurjchem-1080	9	48	rp‐18e	rp‐18e	VERB
eurjchem-1080	9	49	(	(	PUNCT
eurjchem-1080	9	50	100	100	NUM
eurjchem-1080	9	51	×	×	NOUN
eurjchem-1080	9	52	4.6	4.6	NUM
eurjchem-1080	9	53	mm	mm	NOUN
eurjchem-1080	9	54	,	,	PUNCT
eurjchem-1080	9	55	i.d	i.d	PROPN
eurjchem-1080	9	56	.	.	PROPN
eurjchem-1080	9	57	;	;	PUNCT
eurjchem-1080	9	58	macropore	macropore	NOUN
eurjchem-1080	9	59	diameter	diameter	NOUN
eurjchem-1080	9	60	,	,	PUNCT
eurjchem-1080	9	61	2	2	NUM
eurjchem-1080	9	62	µm	µm	NOUN
eurjchem-1080	9	63	)	)	PUNCT
eurjchem-1080	9	64	columns	column	NOUN
eurjchem-1080	9	65	using	use	VERB
eurjchem-1080	9	66	a	a	DET
eurjchem-1080	9	67	mobile	mobile	ADJ
eurjchem-1080	9	68	phase	phase	NOUN
eurjchem-1080	9	69	consisting	consist	VERB
eurjchem-1080	9	70	of	of	ADP
eurjchem-1080	9	71	methanol	methanol	NOUN
eurjchem-1080	9	72	:	:	PUNCT
eurjchem-1080	9	73	water	water	NOUN
eurjchem-1080	9	74	:	:	PUNCT
eurjchem-1080	9	75	triethylamine	triethylamine	NOUN
eurjchem-1080	9	76	:	:	PUNCT
eurjchem-1080	9	77	acetic	acetic	ADJ
eurjchem-1080	9	78	acid	acid	NOUN
eurjchem-1080	9	79	(	(	PUNCT
eurjchem-1080	9	80	60:40:0.1:0.1	60:40:0.1:0.1	NOUN
eurjchem-1080	9	81	;	;	PUNCT
eurjchem-1080	9	82	v	v	X
eurjchem-1080	9	83	:	:	PUNCT
eurjchem-1080	9	84	v	v	NOUN
eurjchem-1080	9	85	:	:	PUNCT
eurjchem-1080	9	86	v	v	ADJ
eurjchem-1080	9	87	:	:	PUNCT
eurjchem-1080	9	88	v	v	NOUN
eurjchem-1080	9	89	)	)	PUNCT
eurjchem-1080	9	90	,	,	PUNCT
eurjchem-1080	9	91	at	at	ADP
eurjchem-1080	9	92	a	a	DET
eurjchem-1080	9	93	flow	flow	NOUN
eurjchem-1080	9	94	rate	rate	NOUN
eurjchem-1080	9	95	0.5	0.5	NUM
eurjchem-1080	9	96	ml	ml	NOUN
eurjchem-1080	9	97	/	/	SYM
eurjchem-1080	9	98	min	min	NOUN
eurjchem-1080	9	99	and	and	CCONJ
eurjchem-1080	9	100	uv	uv	NOUN
eurjchem-1080	9	101	detection	detection	NOUN
eurjchem-1080	9	102	at	at	ADP
eurjchem-1080	9	103	268	268	NUM
eurjchem-1080	9	104	nm	nm	NOUN
eurjchem-1080	9	105	.	.	PUNCT
eurjchem-1080	10	1	the	the	DET
eurjchem-1080	10	2	method	method	NOUN
eurjchem-1080	10	3	was	be	AUX
eurjchem-1080	10	4	linear	linear	ADJ
eurjchem-1080	10	5	over	over	ADP
eurjchem-1080	10	6	the	the	DET
eurjchem-1080	10	7	concentration	concentration	NOUN
eurjchem-1080	10	8	range	range	NOUN
eurjchem-1080	10	9	of	of	ADP
eurjchem-1080	10	10	100‐1000	100‐1000	NUM
eurjchem-1080	10	11	µg	µg	NOUN
eurjchem-1080	10	12	/	/	SYM
eurjchem-1080	10	13	ml	ml	NOUN
eurjchem-1080	10	14	(	(	PUNCT
eurjchem-1080	10	15	r	r	NOUN
eurjchem-1080	10	16	=	=	SYM
eurjchem-1080	10	17	0.9998	0.9998	NUM
eurjchem-1080	10	18	)	)	PUNCT
eurjchem-1080	10	19	with	with	ADP
eurjchem-1080	10	20	a	a	DET
eurjchem-1080	10	21	limit	limit	NOUN
eurjchem-1080	10	22	of	of	ADP
eurjchem-1080	10	23	detection	detection	NOUN
eurjchem-1080	10	24	and	and	CCONJ
eurjchem-1080	10	25	quantitation	quantitation	NOUN
eurjchem-1080	10	26	of	of	ADP
eurjchem-1080	10	27	10	10	NUM
eurjchem-1080	10	28	and	and	CCONJ
eurjchem-1080	10	29	30	30	NUM
eurjchem-1080	10	30	µg	µg	NOUN
eurjchem-1080	10	31	/	/	SYM
eurjchem-1080	10	32	ml	ml	NOUN
eurjchem-1080	10	33	,	,	PUNCT
eurjchem-1080	10	34	respectively	respectively	ADV
eurjchem-1080	10	35	.	.	PUNCT
eurjchem-1080	11	1	all	all	DET
eurjchem-1080	11	2	the	the	DET
eurjchem-1080	11	3	validation	validation	NOUN
eurjchem-1080	11	4	parameters	parameter	NOUN
eurjchem-1080	11	5	and	and	CCONJ
eurjchem-1080	11	6	stability	stability	NOUN
eurjchem-1080	11	7	indicating	indicate	VERB
eurjchem-1080	11	8	study	study	NOUN
eurjchem-1080	11	9	were	be	AUX
eurjchem-1080	11	10	studied	study	VERB
eurjchem-1080	11	11	on	on	ADP
eurjchem-1080	11	12	poroshell	poroshell	PROPN
eurjchem-1080	11	13	120	120	NUM
eurjchem-1080	11	14	ec‐c18	ec‐c18	NOUN
eurjchem-1080	11	15	column	column	NOUN
eurjchem-1080	11	16	,	,	PUNCT
eurjchem-1080	11	17	which	which	PRON
eurjchem-1080	11	18	achieved	achieve	VERB
eurjchem-1080	11	19	the	the	DET
eurjchem-1080	11	20	best	good	ADJ
eurjchem-1080	11	21	separation	separation	NOUN
eurjchem-1080	11	22	.	.	PUNCT
eurjchem-1080	12	1	the	the	DET
eurjchem-1080	12	2	proposed	propose	VERB
eurjchem-1080	12	3	method	method	NOUN
eurjchem-1080	12	4	has	have	AUX
eurjchem-1080	12	5	been	be	AUX
eurjchem-1080	12	6	found	find	VERB
eurjchem-1080	12	7	to	to	PART
eurjchem-1080	12	8	have	have	VERB
eurjchem-1080	12	9	the	the	DET
eurjchem-1080	12	10	required	require	VERB
eurjchem-1080	12	11	accuracy	accuracy	NOUN
eurjchem-1080	12	12	,	,	PUNCT
eurjchem-1080	12	13	selectivity	selectivity	NOUN
eurjchem-1080	12	14	,	,	PUNCT
eurjchem-1080	12	15	sensitivity	sensitivity	NOUN
eurjchem-1080	12	16	,	,	PUNCT
eurjchem-1080	12	17	and	and	CCONJ
eurjchem-1080	12	18	precision	precision	NOUN
eurjchem-1080	12	19	to	to	PART
eurjchem-1080	12	20	assay	assay	VERB
eurjchem-1080	12	21	sitagliptin	sitagliptin	NOUN
eurjchem-1080	12	22	phosphate	phosphate	NOUN
eurjchem-1080	12	23	in	in	ADP
eurjchem-1080	12	24	bulk	bulk	ADJ
eurjchem-1080	12	25	form	form	NOUN
eurjchem-1080	12	26	and	and	CCONJ
eurjchem-1080	12	27	in	in	ADP
eurjchem-1080	12	28	a	a	DET
eurjchem-1080	12	29	pharmaceutical	pharmaceutical	ADJ
eurjchem-1080	12	30	dosage	dosage	NOUN
eurjchem-1080	12	31	form	form	NOUN
eurjchem-1080	12	32	.	.	PUNCT
eurjchem-1080	13	1	degradation	degradation	NOUN
eurjchem-1080	13	2	products	product	NOUN
eurjchem-1080	13	3	resulting	result	VERB
eurjchem-1080	13	4	from	from	ADP
eurjchem-1080	13	5	the	the	DET
eurjchem-1080	13	6	stress	stress	NOUN
eurjchem-1080	13	7	studies	study	NOUN
eurjchem-1080	13	8	did	do	AUX
eurjchem-1080	13	9	not	not	PART
eurjchem-1080	13	10	interfere	interfere	VERB
eurjchem-1080	13	11	with	with	ADP
eurjchem-1080	13	12	the	the	DET
eurjchem-1080	13	13	detection	detection	NOUN
eurjchem-1080	13	14	of	of	ADP
eurjchem-1080	13	15	sitagliptin	sitagliptin	NOUN
eurjchem-1080	13	16	phosphate	phosphate	NOUN
eurjchem-1080	13	17	that	that	PRON
eurjchem-1080	13	18	indicates	indicate	VERB
eurjchem-1080	13	19	that	that	SCONJ
eurjchem-1080	13	20	the	the	DET
eurjchem-1080	13	21	assay	assay	NOUN
eurjchem-1080	13	22	are	be	AUX
eurjchem-1080	13	23	stability‐indicating	stability‐indicate	VERB
eurjchem-1080	13	24	assay	assay	NOUN
eurjchem-1080	13	25	.	.	PUNCT
eurjchem-1080	14	1	hplc	hplc	PROPN
eurjchem-1080	14	2	sitagliptin	sitagliptin	PROPN
eurjchem-1080	14	3	sitagliptin	sitagliptin	PROPN
eurjchem-1080	14	4	phosphate	phosphate	ADJ
eurjchem-1080	14	5	liquid	liquid	NOUN
eurjchem-1080	14	6	chromatography	chromatography	NOUN
eurjchem-1080	14	7	stability‐indicating	stability‐indicate	VERB
eurjchem-1080	14	8	assays	assay	NOUN
eurjchem-1080	14	9	pharmaceutical	pharmaceutical	ADJ
eurjchem-1080	14	10	dosage	dosage	NOUN
eurjchem-1080	14	11	form	form	NOUN
eurjchem-1080	14	12	1	1	NUM
eurjchem-1080	14	13	.	.	PUNCT
eurjchem-1080	14	14	introduction	introduction	NOUN
eurjchem-1080	14	15	sitagliptin	sitagliptin	NOUN
eurjchem-1080	14	16	phosphate	phosphate	NOUN
eurjchem-1080	14	17	(	(	PUNCT
eurjchem-1080	14	18	stg	stg	NOUN
eurjchem-1080	14	19	)	)	PUNCT
eurjchem-1080	15	1	[	[	X
eurjchem-1080	15	2	1‐4	1‐4	NOUN
eurjchem-1080	15	3	]	]	X
eurjchem-1080	15	4	is	be	AUX
eurjchem-1080	15	5	1,2,4‐triazolo	1,2,4‐triazolo	NUM
eurjchem-1080	16	1	[	[	X
eurjchem-1080	16	2	4,3‐a	4,3‐a	X
eurjchem-1080	16	3	]	]	X
eurjchem-1080	16	4	pyrazine,7‐[(3r)‐3‐amino‐1‐oxo‐4‐(2,4,5‐trifluorophenyl	pyrazine,7‐[(3r)‐3‐amino‐1‐oxo‐4‐(2,4,5‐trifluorophenyl	PROPN
eurjchem-1080	16	5	)	)	PUNCT
eurjchem-1080	16	6	butyl]‐5,6,7,8‐tetra‐hydro‐3‐(trifluoromethyl	butyl]‐5,6,7,8‐tetra‐hydro‐3‐(trifluoromethyl	PROPN
eurjchem-1080	16	7	)	)	PUNCT
eurjchem-1080	16	8	phosphate	phosphate	NOUN
eurjchem-1080	16	9	(	(	PUNCT
eurjchem-1080	16	10	figure	figure	NOUN
eurjchem-1080	16	11	1	1	NUM
eurjchem-1080	16	12	)	)	PUNCT
eurjchem-1080	16	13	.	.	PUNCT
eurjchem-1080	17	1	it	it	PRON
eurjchem-1080	17	2	is	be	AUX
eurjchem-1080	17	3	the	the	DET
eurjchem-1080	17	4	first	first	ADJ
eurjchem-1080	17	5	dipeptidylpeptidase‐4	dipeptidylpeptidase‐4	ADJ
eurjchem-1080	17	6	inhibitor	inhibitor	NOUN
eurjchem-1080	17	7	to	to	PART
eurjchem-1080	17	8	be	be	AUX
eurjchem-1080	17	9	used	use	VERB
eurjchem-1080	17	10	in	in	ADP
eurjchem-1080	17	11	the	the	DET
eurjchem-1080	17	12	management	management	NOUN
eurjchem-1080	17	13	of	of	ADP
eurjchem-1080	17	14	type	type	NOUN
eurjchem-1080	17	15	2	2	NUM
eurjchem-1080	17	16	diabetes	diabetes	NOUN
eurjchem-1080	17	17	.	.	PUNCT
eurjchem-1080	18	1	it	it	PRON
eurjchem-1080	18	2	is	be	AUX
eurjchem-1080	18	3	widely	widely	ADV
eurjchem-1080	18	4	used	use	VERB
eurjchem-1080	18	5	as	as	ADP
eurjchem-1080	18	6	an	an	DET
eurjchem-1080	18	7	add‐on	add‐on	PROPN
eurjchem-1080	18	8	therapy	therapy	NOUN
eurjchem-1080	18	9	to	to	ADP
eurjchem-1080	18	10	ongoing	ongoing	ADJ
eurjchem-1080	18	11	management	management	NOUN
eurjchem-1080	18	12	or	or	CCONJ
eurjchem-1080	18	13	as	as	ADP
eurjchem-1080	18	14	monotherapy	monotherapy	NOUN
eurjchem-1080	18	15	when	when	SCONJ
eurjchem-1080	18	16	it	it	PRON
eurjchem-1080	18	17	is	be	AUX
eurjchem-1080	18	18	deemed	deem	VERB
eurjchem-1080	18	19	necessary	necessary	ADJ
eurjchem-1080	18	20	.	.	PUNCT
eurjchem-1080	19	1	it	it	PRON
eurjchem-1080	19	2	has	have	AUX
eurjchem-1080	19	3	been	be	AUX
eurjchem-1080	19	4	found	find	VERB
eurjchem-1080	19	5	to	to	PART
eurjchem-1080	19	6	be	be	AUX
eurjchem-1080	19	7	beneficial	beneficial	ADJ
eurjchem-1080	19	8	in	in	ADP
eurjchem-1080	19	9	improving	improve	VERB
eurjchem-1080	19	10	β‐cell	β‐cell	PUNCT
eurjchem-1080	19	11	function	function	NOUN
eurjchem-1080	19	12	and	and	CCONJ
eurjchem-1080	19	13	glycemic	glycemic	ADJ
eurjchem-1080	19	14	control	control	NOUN
eurjchem-1080	19	15	.	.	PUNCT
eurjchem-1080	20	1	moreover	moreover	ADV
eurjchem-1080	20	2	,	,	PUNCT
eurjchem-1080	20	3	in	in	ADP
eurjchem-1080	20	4	special	special	ADJ
eurjchem-1080	20	5	circumstances	circumstance	NOUN
eurjchem-1080	20	6	like	like	ADP
eurjchem-1080	20	7	chronic	chronic	ADJ
eurjchem-1080	20	8	kidney	kidney	NOUN
eurjchem-1080	20	9	disease	disease	NOUN
eurjchem-1080	20	10	it	it	PRON
eurjchem-1080	20	11	is	be	AUX
eurjchem-1080	20	12	used	use	VERB
eurjchem-1080	20	13	with	with	ADP
eurjchem-1080	20	14	appropriate	appropriate	ADJ
eurjchem-1080	20	15	dose	dose	NOUN
eurjchem-1080	20	16	reductions	reduction	NOUN
eurjchem-1080	20	17	[	[	X
eurjchem-1080	20	18	5	5	NUM
eurjchem-1080	20	19	]	]	PUNCT
eurjchem-1080	20	20	.	.	PUNCT
eurjchem-1080	21	1	literature	literature	NOUN
eurjchem-1080	21	2	survey	survey	NOUN
eurjchem-1080	21	3	revealed	reveal	VERB
eurjchem-1080	21	4	that	that	SCONJ
eurjchem-1080	21	5	some	some	DET
eurjchem-1080	21	6	lc‐ms	lc‐ms	NOUN
eurjchem-1080	21	7	methods	method	NOUN
eurjchem-1080	21	8	[	[	X
eurjchem-1080	21	9	6‐9	6‐9	NOUN
eurjchem-1080	21	10	]	]	PUNCT
eurjchem-1080	21	11	were	be	AUX
eurjchem-1080	21	12	reported	report	VERB
eurjchem-1080	21	13	for	for	ADP
eurjchem-1080	21	14	the	the	DET
eurjchem-1080	21	15	determination	determination	NOUN
eurjchem-1080	21	16	of	of	ADP
eurjchem-1080	21	17	sitagliptin	sitagliptin	NOUN
eurjchem-1080	21	18	phosphate	phosphate	NOUN
eurjchem-1080	21	19	in	in	ADP
eurjchem-1080	21	20	plasma	plasma	NOUN
eurjchem-1080	21	21	and	and	CCONJ
eurjchem-1080	21	22	urine	urine	NOUN
eurjchem-1080	21	23	of	of	ADP
eurjchem-1080	21	24	humans	human	NOUN
eurjchem-1080	21	25	,	,	PUNCT
eurjchem-1080	21	26	rats	rat	NOUN
eurjchem-1080	21	27	and	and	CCONJ
eurjchem-1080	21	28	dogs	dog	NOUN
eurjchem-1080	21	29	.	.	PUNCT
eurjchem-1080	22	1	also	also	ADV
eurjchem-1080	22	2	,	,	PUNCT
eurjchem-1080	22	3	spectrophoto‐	spectrophoto‐	PROPN
eurjchem-1080	22	4	metric	metric	ADJ
eurjchem-1080	22	5	techniques	technique	NOUN
eurjchem-1080	22	6	were	be	AUX
eurjchem-1080	22	7	used	use	VERB
eurjchem-1080	22	8	for	for	ADP
eurjchem-1080	22	9	the	the	DET
eurjchem-1080	22	10	determination	determination	NOUN
eurjchem-1080	22	11	of	of	ADP
eurjchem-1080	22	12	sitagliptin	sitagliptin	NOUN
eurjchem-1080	22	13	and	and	CCONJ
eurjchem-1080	22	14	characterized	characterize	VERB
eurjchem-1080	22	15	by	by	ADP
eurjchem-1080	22	16	their	their	PRON
eurjchem-1080	22	17	simplicity	simplicity	NOUN
eurjchem-1080	22	18	,	,	PUNCT
eurjchem-1080	22	19	specificity	specificity	NOUN
eurjchem-1080	22	20	and	and	CCONJ
eurjchem-1080	22	21	low	low	ADJ
eurjchem-1080	22	22	cost	cost	NOUN
eurjchem-1080	22	23	[	[	X
eurjchem-1080	22	24	10,11	10,11	NOUN
eurjchem-1080	22	25	]	]	PUNCT
eurjchem-1080	22	26	.	.	PUNCT
eurjchem-1080	23	1	in	in	ADP
eurjchem-1080	23	2	addition	addition	NOUN
eurjchem-1080	23	3	,	,	PUNCT
eurjchem-1080	23	4	some	some	DET
eurjchem-1080	23	5	analytical	analytical	ADJ
eurjchem-1080	23	6	methods	method	NOUN
eurjchem-1080	23	7	were	be	AUX
eurjchem-1080	23	8	used	use	VERB
eurjchem-1080	23	9	for	for	ADP
eurjchem-1080	23	10	the	the	DET
eurjchem-1080	23	11	validation	validation	NOUN
eurjchem-1080	23	12	and	and	CCONJ
eurjchem-1080	23	13	estimation	estimation	NOUN
eurjchem-1080	23	14	of	of	ADP
eurjchem-1080	23	15	sitagliptin	sitagliptin	NOUN
eurjchem-1080	23	16	in	in	ADP
eurjchem-1080	23	17	bulk	bulk	NOUN
eurjchem-1080	23	18	and	and	CCONJ
eurjchem-1080	23	19	pharmaceutical	pharmaceutical	NOUN
eurjchem-1080	23	20	formulations	formulation	NOUN
eurjchem-1080	23	21	[	[	X
eurjchem-1080	23	22	12‐14	12‐14	X
eurjchem-1080	23	23	]	]	PUNCT
eurjchem-1080	23	24	.	.	PUNCT
eurjchem-1080	24	1	this	this	DET
eurjchem-1080	24	2	study	study	NOUN
eurjchem-1080	24	3	presents	present	VERB
eurjchem-1080	24	4	a	a	DET
eurjchem-1080	24	5	comparative	comparative	ADJ
eurjchem-1080	24	6	determination	determination	NOUN
eurjchem-1080	24	7	of	of	ADP
eurjchem-1080	24	8	sitagliptin	sitagliptin	NOUN
eurjchem-1080	24	9	phosphate	phosphate	NOUN
eurjchem-1080	24	10	on	on	ADP
eurjchem-1080	24	11	three	three	NUM
eurjchem-1080	24	12	different	different	ADJ
eurjchem-1080	24	13	stationary	stationary	ADJ
eurjchem-1080	24	14	phases	phase	NOUN
eurjchem-1080	24	15	,	,	PUNCT
eurjchem-1080	24	16	poroshell	poroshell	VERB
eurjchem-1080	24	17	120	120	NUM
eurjchem-1080	24	18	ec‐c18	ec‐c18	NOUN
eurjchem-1080	24	19	,	,	PUNCT
eurjchem-1080	24	20	pursuit	pursuit	NOUN
eurjchem-1080	24	21	5pfp	5pfp	NUM
eurjchem-1080	24	22	and	and	CCONJ
eurjchem-1080	24	23	chromolith	chromolith	NOUN
eurjchem-1080	24	24	performance	performance	NOUN
eurjchem-1080	24	25	rp‐18e	rp‐18e	VERB
eurjchem-1080	24	26	column	column	NOUN
eurjchem-1080	24	27	.	.	PUNCT
eurjchem-1080	25	1	all	all	DET
eurjchem-1080	25	2	the	the	DET
eurjchem-1080	25	3	validation	validation	NOUN
eurjchem-1080	25	4	parameters	parameter	NOUN
eurjchem-1080	25	5	and	and	CCONJ
eurjchem-1080	25	6	stability‐indicating	stability‐indicate	VERB
eurjchem-1080	25	7	study	study	NOUN
eurjchem-1080	25	8	will	will	AUX
eurjchem-1080	25	9	be	be	AUX
eurjchem-1080	25	10	studied	study	VERB
eurjchem-1080	25	11	on	on	ADP
eurjchem-1080	25	12	the	the	DET
eurjchem-1080	25	13	column	column	NOUN
eurjchem-1080	25	14	,	,	PUNCT
eurjchem-1080	25	15	which	which	PRON
eurjchem-1080	25	16	achieves	achieve	VERB
eurjchem-1080	25	17	the	the	DET
eurjchem-1080	25	18	best	good	ADJ
eurjchem-1080	25	19	determination	determination	NOUN
eurjchem-1080	25	20	of	of	ADP
eurjchem-1080	25	21	sitagliptin	sitagliptin	NOUN
eurjchem-1080	25	22	phosphate	phosphate	NOUN
eurjchem-1080	25	23	in	in	ADP
eurjchem-1080	25	24	bulk	bulk	NOUN
eurjchem-1080	25	25	and	and	CCONJ
eurjchem-1080	25	26	pharmaceutical	pharmaceutical	ADJ
eurjchem-1080	25	27	formula‐	formula‐	NUM
eurjchem-1080	25	28	tions	tion	NOUN
eurjchem-1080	25	29	.	.	PUNCT
eurjchem-1080	26	1	figure	figure	NOUN
eurjchem-1080	26	2	1	1	NUM
eurjchem-1080	26	3	.	.	PUNCT
eurjchem-1080	26	4	sitagliptin	sitagliptin	NOUN
eurjchem-1080	26	5	phosphate	phosphate	NOUN
eurjchem-1080	26	6	.	.	PUNCT
eurjchem-1080	27	1	2	2	X
eurjchem-1080	27	2	.	.	X
eurjchem-1080	27	3	experimental	experimental	ADJ
eurjchem-1080	27	4	2.1	2.1	NUM
eurjchem-1080	27	5	.	.	PUNCT
eurjchem-1080	27	6	chemicals	chemical	NOUN
eurjchem-1080	27	7	and	and	CCONJ
eurjchem-1080	27	8	reagents	reagent	NOUN
eurjchem-1080	27	9	sitagliptin	sitagliptin	NOUN
eurjchem-1080	27	10	phosphate	phosphate	NOUN
eurjchem-1080	27	11	standard	standard	ADJ
eurjchem-1080	27	12	bulk	bulk	ADJ
eurjchem-1080	27	13	powder	powder	NOUN
eurjchem-1080	27	14	was	be	AUX
eurjchem-1080	27	15	obtained	obtain	VERB
eurjchem-1080	27	16	from	from	ADP
eurjchem-1080	27	17	merck	merck	PROPN
eurjchem-1080	27	18	sharp	sharp	PROPN
eurjchem-1080	27	19	&	&	CCONJ
eurjchem-1080	27	20	dohme	dohme	PROPN
eurjchem-1080	27	21	ltd	ltd	PROPN
eurjchem-1080	27	22	.	.	PROPN
eurjchem-1080	27	23	,	,	PUNCT
eurjchem-1080	27	24	cramlington	cramlington	PROPN
eurjchem-1080	27	25	northumberland	northumberland	PROPN
eurjchem-1080	27	26	and	and	CCONJ
eurjchem-1080	27	27	was	be	AUX
eurjchem-1080	27	28	used	use	VERB
eurjchem-1080	27	29	as	as	SCONJ
eurjchem-1080	27	30	received	receive	VERB
eurjchem-1080	27	31	,	,	PUNCT
eurjchem-1080	27	32	certified	certify	VERB
eurjchem-1080	27	33	to	to	PART
eurjchem-1080	27	34	be	be	AUX
eurjchem-1080	27	35	99.80	99.80	NUM
eurjchem-1080	27	36	%	%	NOUN
eurjchem-1080	27	37	pure	pure	ADJ
eurjchem-1080	27	38	.	.	PUNCT
eurjchem-1080	28	1	januvia	januvia	PROPN
eurjchem-1080	28	2	100	100	NUM
eurjchem-1080	28	3	mg	mg	PROPN
eurjchem-1080	28	4	,	,	PUNCT
eurjchem-1080	28	5	50	50	NUM
eurjchem-1080	28	6	mg	mg	NOUN
eurjchem-1080	28	7	and	and	CCONJ
eurjchem-1080	28	8	25	25	NUM
eurjchem-1080	28	9	mg	mg	NOUN
eurjchem-1080	28	10	(	(	PUNCT
eurjchem-1080	28	11	labeled	label	VERB
eurjchem-1080	28	12	to	to	PART
eurjchem-1080	28	13	contain	contain	VERB
eurjchem-1080	28	14	100	100	NUM
eurjchem-1080	28	15	mg	mg	NOUN
eurjchem-1080	28	16	,	,	PUNCT
eurjchem-1080	28	17	50	50	NUM
eurjchem-1080	28	18	mg	mg	NOUN
eurjchem-1080	28	19	and	and	CCONJ
eurjchem-1080	28	20	25	25	NUM
eurjchem-1080	28	21	mg	mg	NOUN
eurjchem-1080	28	22	of	of	ADP
eurjchem-1080	28	23	sitagliptin	sitagliptin	NOUN
eurjchem-1080	28	24	phosphate	phosphate	NOUN
eurjchem-1080	28	25	per	per	ADP
eurjchem-1080	28	26	tablet	tablet	NOUN
eurjchem-1080	28	27	)	)	PUNCT
eurjchem-1080	28	28	were	be	AUX
eurjchem-1080	28	29	obtained	obtain	VERB
eurjchem-1080	28	30	from	from	ADP
eurjchem-1080	28	31	the	the	DET
eurjchem-1080	28	32	merck	merck	PROPN
eurjchem-1080	28	33	sharp	sharp	PROPN
eurjchem-1080	28	34	&	&	CCONJ
eurjchem-1080	28	35	dohme	dohme	PROPN
eurjchem-1080	28	36	ltd	ltd	PROPN
eurjchem-1080	28	37	.	.	PROPN
eurjchem-1080	28	38	,	,	PUNCT
eurjchem-1080	28	39	cramlington	cramlington	PROPN
eurjchem-1080	28	40	,	,	PUNCT
eurjchem-1080	28	41	uk	uk	PROPN
eurjchem-1080	28	42	498	498	NUM
eurjchem-1080	28	43	saleh	saleh	NOUN
eurjchem-1080	28	44	et	et	PROPN
eurjchem-1080	28	45	al	al	PROPN
eurjchem-1080	28	46	.	.	PUNCT
eurjchem-1080	28	47	/	/	SYM
eurjchem-1080	28	48	european	european	PROPN
eurjchem-1080	28	49	journal	journal	PROPN
eurjchem-1080	28	50	of	of	ADP
eurjchem-1080	28	51	chemistry	chemistry	NOUN
eurjchem-1080	28	52	5	5	NUM
eurjchem-1080	28	53	(	(	PUNCT
eurjchem-1080	28	54	3	3	NUM
eurjchem-1080	28	55	)	)	PUNCT
eurjchem-1080	28	56	(	(	PUNCT
eurjchem-1080	28	57	2014	2014	NUM
eurjchem-1080	28	58	)	)	PUNCT
eurjchem-1080	28	59	497‐502	497‐502	PROPN
eurjchem-1080	28	60	(	(	PUNCT
eurjchem-1080	28	61	imported	import	VERB
eurjchem-1080	28	62	by	by	ADP
eurjchem-1080	28	63	soficopharm	soficopharm	NOUN
eurjchem-1080	28	64	,	,	PUNCT
eurjchem-1080	28	65	cairo	cairo	PROPN
eurjchem-1080	28	66	,	,	PUNCT
eurjchem-1080	28	67	egypt	egypt	PROPN
eurjchem-1080	28	68	)	)	PUNCT
eurjchem-1080	28	69	.	.	PUNCT
eurjchem-1080	29	1	methanol	methanol	NOUN
eurjchem-1080	29	2	,	,	PUNCT
eurjchem-1080	29	3	triethyl	triethyl	PROPN
eurjchem-1080	29	4	amine	amine	NOUN
eurjchem-1080	29	5	,	,	PUNCT
eurjchem-1080	29	6	acetic	acetic	ADJ
eurjchem-1080	29	7	acid	acid	NOUN
eurjchem-1080	29	8	were	be	AUX
eurjchem-1080	29	9	obtained	obtain	VERB
eurjchem-1080	29	10	from	from	ADP
eurjchem-1080	29	11	merck	merck	PROPN
eurjchem-1080	29	12	(	(	PUNCT
eurjchem-1080	29	13	darmstadt	darmstadt	PROPN
eurjchem-1080	29	14	,	,	PUNCT
eurjchem-1080	29	15	germany	germany	PROPN
eurjchem-1080	29	16	)	)	PUNCT
eurjchem-1080	29	17	.	.	PUNCT
eurjchem-1080	30	1	all	all	DET
eurjchem-1080	30	2	chemicals	chemical	NOUN
eurjchem-1080	30	3	were	be	AUX
eurjchem-1080	30	4	of	of	ADP
eurjchem-1080	30	5	analytical	analytical	ADJ
eurjchem-1080	30	6	grade	grade	NOUN
eurjchem-1080	30	7	.	.	PUNCT
eurjchem-1080	31	1	purified	purified	ADJ
eurjchem-1080	31	2	hplc	hplc	NOUN
eurjchem-1080	31	3	grade	grade	NOUN
eurjchem-1080	31	4	water	water	NOUN
eurjchem-1080	31	5	was	be	AUX
eurjchem-1080	31	6	obtained	obtain	VERB
eurjchem-1080	31	7	by	by	ADP
eurjchem-1080	31	8	reverse	reverse	ADJ
eurjchem-1080	31	9	osmosis	osmosis	NOUN
eurjchem-1080	31	10	and	and	CCONJ
eurjchem-1080	31	11	filtration	filtration	NOUN
eurjchem-1080	31	12	through	through	ADP
eurjchem-1080	31	13	a	a	DET
eurjchem-1080	31	14	milli‐q	milli‐q	NOUN
eurjchem-1080	31	15	system	system	NOUN
eurjchem-1080	31	16	(	(	PUNCT
eurjchem-1080	31	17	millipore	millipore	PROPN
eurjchem-1080	31	18	,	,	PUNCT
eurjchem-1080	31	19	milfored	milfore	VERB
eurjchem-1080	31	20	,	,	PUNCT
eurjchem-1080	31	21	ma	ma	PROPN
eurjchem-1080	31	22	,	,	PUNCT
eurjchem-1080	31	23	usa	usa	PROPN
eurjchem-1080	31	24	)	)	PUNCT
eurjchem-1080	31	25	and	and	CCONJ
eurjchem-1080	31	26	was	be	AUX
eurjchem-1080	31	27	used	use	VERB
eurjchem-1080	31	28	as	as	ADP
eurjchem-1080	31	29	a	a	DET
eurjchem-1080	31	30	mobile	mobile	ADJ
eurjchem-1080	31	31	phase	phase	NOUN
eurjchem-1080	31	32	.	.	PUNCT
eurjchem-1080	32	1	2.2	2.2	NUM
eurjchem-1080	32	2	.	.	PUNCT
eurjchem-1080	32	3	instrumentation	instrumentation	NOUN
eurjchem-1080	32	4	and	and	CCONJ
eurjchem-1080	32	5	conditions	condition	NOUN
eurjchem-1080	32	6	the	the	DET
eurjchem-1080	32	7	hplc	hplc	NOUN
eurjchem-1080	32	8	unit	unit	NOUN
eurjchem-1080	32	9	was	be	AUX
eurjchem-1080	32	10	an	an	DET
eurjchem-1080	32	11	agilent	agilent	PROPN
eurjchem-1080	32	12	1100	1100	NUM
eurjchem-1080	32	13	series	series	NOUN
eurjchem-1080	32	14	apparatus	apparatus	NOUN
eurjchem-1080	32	15	equipped	equip	VERB
eurjchem-1080	32	16	with	with	ADP
eurjchem-1080	32	17	a	a	DET
eurjchem-1080	32	18	quaternary	quaternary	ADJ
eurjchem-1080	32	19	pump	pump	NOUN
eurjchem-1080	32	20	,	,	PUNCT
eurjchem-1080	32	21	a	a	DET
eurjchem-1080	32	22	vacuum	vacuum	NOUN
eurjchem-1080	32	23	degasser	degasser	NOUN
eurjchem-1080	32	24	,	,	PUNCT
eurjchem-1080	32	25	a	a	DET
eurjchem-1080	32	26	column	column	NOUN
eurjchem-1080	32	27	oven	oven	VERB
eurjchem-1080	32	28	,	,	PUNCT
eurjchem-1080	32	29	a	a	DET
eurjchem-1080	32	30	diode	diode	NOUN
eurjchem-1080	32	31	array	array	NOUN
eurjchem-1080	32	32	uv‐detector	uv‐detector	NOUN
eurjchem-1080	32	33	and	and	CCONJ
eurjchem-1080	32	34	hp	hp	ADJ
eurjchem-1080	32	35	chemstation	chemstation	NOUN
eurjchem-1080	32	36	for	for	ADP
eurjchem-1080	32	37	lc	lc	PROPN
eurjchem-1080	32	38	3d	3d	PROPN
eurjchem-1080	32	39	systems	system	NOUN
eurjchem-1080	32	40	b.0301	b.0301	NOUN
eurjchem-1080	33	1	[	[	X
eurjchem-1080	33	2	317	317	NUM
eurjchem-1080	33	3	]	]	ADJ
eurjchem-1080	33	4	software	software	NOUN
eurjchem-1080	33	5	.	.	PUNCT
eurjchem-1080	34	1	three	three	NUM
eurjchem-1080	34	2	columns	column	NOUN
eurjchem-1080	34	3	were	be	AUX
eurjchem-1080	34	4	used	use	VERB
eurjchem-1080	34	5	in	in	ADP
eurjchem-1080	34	6	this	this	DET
eurjchem-1080	34	7	study	study	NOUN
eurjchem-1080	34	8	namely	namely	ADV
eurjchem-1080	34	9	(	(	PUNCT
eurjchem-1080	34	10	100	100	NUM
eurjchem-1080	34	11	×	×	NOUN
eurjchem-1080	34	12	4.6	4.6	NUM
eurjchem-1080	34	13	mm	mm	NOUN
eurjchem-1080	34	14	,	,	PUNCT
eurjchem-1080	34	15	i.d	i.d	PROPN
eurjchem-1080	34	16	.	.	PROPN
eurjchem-1080	34	17	;	;	PUNCT
eurjchem-1080	34	18	particle	particle	NOUN
eurjchem-1080	34	19	size	size	NOUN
eurjchem-1080	34	20	,	,	PUNCT
eurjchem-1080	34	21	2.7	2.7	NUM
eurjchem-1080	34	22	µm	µm	NOUN
eurjchem-1080	34	23	)	)	PUNCT
eurjchem-1080	34	24	,	,	PUNCT
eurjchem-1080	34	25	pursuit	pursuit	VERB
eurjchem-1080	34	26	5pfp	5pfp	NUM
eurjchem-1080	34	27	(	(	PUNCT
eurjchem-1080	34	28	150	150	NUM
eurjchem-1080	34	29	×	×	NOUN
eurjchem-1080	34	30	4.6	4.6	NUM
eurjchem-1080	34	31	mm	mm	NOUN
eurjchem-1080	34	32	,	,	PUNCT
eurjchem-1080	34	33	i.d	i.d	PROPN
eurjchem-1080	34	34	.	.	PROPN
eurjchem-1080	34	35	;	;	PUNCT
eurjchem-1080	34	36	particle	particle	NOUN
eurjchem-1080	34	37	size	size	NOUN
eurjchem-1080	34	38	,	,	PUNCT
eurjchem-1080	34	39	5	5	NUM
eurjchem-1080	34	40	µm	µm	NOUN
eurjchem-1080	34	41	)	)	PUNCT
eurjchem-1080	34	42	were	be	AUX
eurjchem-1080	34	43	purchased	purchase	VERB
eurjchem-1080	34	44	from	from	ADP
eurjchem-1080	34	45	agilent	agilent	PROPN
eurjchem-1080	34	46	technologies	technology	NOUN
eurjchem-1080	34	47	and	and	CCONJ
eurjchem-1080	34	48	(	(	PUNCT
eurjchem-1080	34	49	100	100	NUM
eurjchem-1080	34	50	×	×	NOUN
eurjchem-1080	34	51	4.6	4.6	NUM
eurjchem-1080	34	52	mm	mm	NOUN
eurjchem-1080	34	53	,	,	PUNCT
eurjchem-1080	34	54	i.d	i.d	PROPN
eurjchem-1080	34	55	.	.	PROPN
eurjchem-1080	34	56	;	;	PUNCT
eurjchem-1080	34	57	macropore	macropore	NOUN
eurjchem-1080	34	58	diameter	diameter	NOUN
eurjchem-1080	34	59	,	,	PUNCT
eurjchem-1080	34	60	2	2	NUM
eurjchem-1080	34	61	µm	µm	NOUN
eurjchem-1080	34	62	)	)	PUNCT
eurjchem-1080	34	63	was	be	AUX
eurjchem-1080	34	64	from	from	ADP
eurjchem-1080	34	65	merck	merck	PROPN
eurjchem-1080	34	66	(	(	PUNCT
eurjchem-1080	34	67	darmstadt	darmstadt	PROPN
eurjchem-1080	34	68	,	,	PUNCT
eurjchem-1080	34	69	germany	germany	PROPN
eurjchem-1080	34	70	)	)	PUNCT
eurjchem-1080	34	71	.	.	PUNCT
eurjchem-1080	35	1	separation	separation	NOUN
eurjchem-1080	35	2	was	be	AUX
eurjchem-1080	35	3	achieved	achieve	VERB
eurjchem-1080	35	4	using	use	VERB
eurjchem-1080	35	5	a	a	DET
eurjchem-1080	35	6	mobile	mobile	ADJ
eurjchem-1080	35	7	phase	phase	NOUN
eurjchem-1080	35	8	consisting	consist	VERB
eurjchem-1080	35	9	of	of	ADP
eurjchem-1080	35	10	methanol	methanol	NOUN
eurjchem-1080	35	11	:	:	PUNCT
eurjchem-1080	35	12	water	water	NOUN
eurjchem-1080	35	13	:	:	PUNCT
eurjchem-1080	35	14	triethylamine	triethylamine	NOUN
eurjchem-1080	35	15	:	:	PUNCT
eurjchem-1080	35	16	acetic	acetic	ADJ
eurjchem-1080	35	17	acid	acid	NOUN
eurjchem-1080	35	18	(	(	PUNCT
eurjchem-1080	35	19	60:40	60:40	NUM
eurjchem-1080	35	20	:	:	PUNCT
eurjchem-1080	35	21	0.1:0.1	0.1:0.1	NUM
eurjchem-1080	35	22	;	;	PUNCT
eurjchem-1080	35	23	v	v	X
eurjchem-1080	35	24	:	:	PUNCT
eurjchem-1080	35	25	v	v	NOUN
eurjchem-1080	35	26	:	:	PUNCT
eurjchem-1080	35	27	v	v	ADJ
eurjchem-1080	35	28	:	:	PUNCT
eurjchem-1080	35	29	v	v	NOUN
eurjchem-1080	35	30	)	)	PUNCT
eurjchem-1080	35	31	,	,	PUNCT
eurjchem-1080	35	32	at	at	ADP
eurjchem-1080	35	33	a	a	DET
eurjchem-1080	35	34	flow	flow	NOUN
eurjchem-1080	35	35	rate	rate	NOUN
eurjchem-1080	35	36	0.5	0.5	NUM
eurjchem-1080	35	37	ml	ml	NOUN
eurjchem-1080	35	38	/	/	SYM
eurjchem-1080	35	39	min	min	NOUN
eurjchem-1080	35	40	.	.	PUNCT
eurjchem-1080	36	1	the	the	DET
eurjchem-1080	36	2	column	column	NOUN
eurjchem-1080	36	3	was	be	AUX
eurjchem-1080	36	4	maintained	maintain	VERB
eurjchem-1080	36	5	at	at	ADP
eurjchem-1080	36	6	temperature	temperature	NOUN
eurjchem-1080	36	7	20	20	NUM
eurjchem-1080	36	8	°	°	ADP
eurjchem-1080	36	9	c	c	NOUN
eurjchem-1080	36	10	and	and	CCONJ
eurjchem-1080	36	11	uv	uv	PROPN
eurjchem-1080	36	12	268	268	NUM
eurjchem-1080	36	13	nm	nm	NOUN
eurjchem-1080	36	14	and	and	CCONJ
eurjchem-1080	36	15	an	an	DET
eurjchem-1080	36	16	injection	injection	NOUN
eurjchem-1080	36	17	volume	volume	NOUN
eurjchem-1080	36	18	of	of	ADP
eurjchem-1080	36	19	5	5	NUM
eurjchem-1080	36	20	µl	µl	NOUN
eurjchem-1080	36	21	was	be	AUX
eurjchem-1080	36	22	used	use	VERB
eurjchem-1080	36	23	.	.	PUNCT
eurjchem-1080	37	1	the	the	DET
eurjchem-1080	37	2	mobile	mobile	ADJ
eurjchem-1080	37	3	phase	phase	NOUN
eurjchem-1080	37	4	was	be	AUX
eurjchem-1080	37	5	filtered	filter	VERB
eurjchem-1080	37	6	through	through	ADP
eurjchem-1080	37	7	0.45	0.45	NUM
eurjchem-1080	37	8	µm	µm	ADP
eurjchem-1080	37	9	chromtech	chromtech	NOUN
eurjchem-1080	37	10	nylon‐66	nylon‐66	PROPN
eurjchem-1080	37	11	filter	filter	NOUN
eurjchem-1080	37	12	and	and	CCONJ
eurjchem-1080	37	13	degassed	degas	VERB
eurjchem-1080	37	14	in	in	ADP
eurjchem-1080	37	15	an	an	DET
eurjchem-1080	37	16	ultrasonic	ultrasonic	ADJ
eurjchem-1080	37	17	bath	bath	NOUN
eurjchem-1080	37	18	.	.	PUNCT
eurjchem-1080	38	1	for	for	ADP
eurjchem-1080	38	2	analysis	analysis	NOUN
eurjchem-1080	38	3	of	of	ADP
eurjchem-1080	38	4	forced	force	VERB
eurjchem-1080	38	5	degradation	degradation	NOUN
eurjchem-1080	38	6	samples	sample	NOUN
eurjchem-1080	38	7	,	,	PUNCT
eurjchem-1080	38	8	the	the	DET
eurjchem-1080	38	9	photodiode	photodiode	NOUN
eurjchem-1080	38	10	array	array	NOUN
eurjchem-1080	38	11	detector	detector	NOUN
eurjchem-1080	38	12	was	be	AUX
eurjchem-1080	38	13	used	use	VERB
eurjchem-1080	38	14	in	in	ADP
eurjchem-1080	38	15	scan	scan	PROPN
eurjchem-1080	38	16	mode	mode	PROPN
eurjchem-1080	38	17	with	with	ADP
eurjchem-1080	38	18	a	a	DET
eurjchem-1080	38	19	scan	scan	ADJ
eurjchem-1080	38	20	range	range	NOUN
eurjchem-1080	38	21	of	of	ADP
eurjchem-1080	38	22	200‐500	200‐500	PROPN
eurjchem-1080	38	23	nm	nm	NOUN
eurjchem-1080	38	24	.	.	PUNCT
eurjchem-1080	39	1	2.3	2.3	NUM
eurjchem-1080	39	2	.	.	PUNCT
eurjchem-1080	40	1	statistical	statistical	ADJ
eurjchem-1080	40	2	analysis	analysis	NOUN
eurjchem-1080	40	3	linear	linear	ADJ
eurjchem-1080	40	4	regression	regression	NOUN
eurjchem-1080	40	5	of	of	ADP
eurjchem-1080	40	6	the	the	DET
eurjchem-1080	40	7	data	datum	NOUN
eurjchem-1080	40	8	was	be	AUX
eurjchem-1080	40	9	performed	perform	VERB
eurjchem-1080	40	10	by	by	ADP
eurjchem-1080	40	11	using	use	VERB
eurjchem-1080	40	12	statistical	statistical	ADJ
eurjchem-1080	40	13	package	package	NOUN
eurjchem-1080	40	14	for	for	ADP
eurjchem-1080	40	15	social	social	ADJ
eurjchem-1080	40	16	science	science	NOUN
eurjchem-1080	40	17	(	(	PUNCT
eurjchem-1080	40	18	spss	spss	PROPN
eurjchem-1080	40	19	)	)	PUNCT
eurjchem-1080	40	20	program	program	NOUN
eurjchem-1080	40	21	version	version	NOUN
eurjchem-1080	40	22	16	16	NUM
eurjchem-1080	40	23	software	software	NOUN
eurjchem-1080	40	24	(	(	PUNCT
eurjchem-1080	40	25	spss	spss	PROPN
eurjchem-1080	40	26	inc	inc	PROPN
eurjchem-1080	40	27	.	.	PROPN
eurjchem-1080	40	28	,	,	PUNCT
eurjchem-1080	40	29	u.s.a	u.s.a	PROPN
eurjchem-1080	40	30	.	.	PUNCT
eurjchem-1080	40	31	)	)	PUNCT
eurjchem-1080	40	32	.	.	PUNCT
eurjchem-1080	41	1	the	the	DET
eurjchem-1080	41	2	level	level	NOUN
eurjchem-1080	41	3	of	of	ADP
eurjchem-1080	41	4	significance	significance	NOUN
eurjchem-1080	41	5	was	be	AUX
eurjchem-1080	41	6	set	set	VERB
eurjchem-1080	41	7	at	at	ADP
eurjchem-1080	41	8	p	p	NOUN
eurjchem-1080	41	9	≤	≤	NUM
eurjchem-1080	41	10	0.05	0.05	NUM
eurjchem-1080	41	11	.	.	PUNCT
eurjchem-1080	42	1	2.4	2.4	NUM
eurjchem-1080	42	2	.	.	PUNCT
eurjchem-1080	42	3	preparation	preparation	NOUN
eurjchem-1080	42	4	of	of	ADP
eurjchem-1080	42	5	stock	stock	NOUN
eurjchem-1080	42	6	and	and	CCONJ
eurjchem-1080	42	7	standard	standard	ADJ
eurjchem-1080	42	8	solutions	solution	NOUN
eurjchem-1080	42	9	a	a	DET
eurjchem-1080	42	10	stock	stock	NOUN
eurjchem-1080	42	11	solution	solution	NOUN
eurjchem-1080	42	12	of	of	ADP
eurjchem-1080	42	13	sitagliptin	sitagliptin	NOUN
eurjchem-1080	42	14	phosphate	phosphate	NOUN
eurjchem-1080	42	15	(	(	PUNCT
eurjchem-1080	42	16	1	1	NUM
eurjchem-1080	42	17	mg	mg	NUM
eurjchem-1080	42	18	/	/	SYM
eurjchem-1080	42	19	ml	ml	NOUN
eurjchem-1080	42	20	)	)	PUNCT
eurjchem-1080	42	21	was	be	AUX
eurjchem-1080	42	22	prepared	prepare	VERB
eurjchem-1080	42	23	in	in	ADP
eurjchem-1080	42	24	hplc‐grade	hplc‐grade	NOUN
eurjchem-1080	42	25	methanol	methanol	NOUN
eurjchem-1080	42	26	.	.	PUNCT
eurjchem-1080	43	1	the	the	DET
eurjchem-1080	43	2	stock	stock	NOUN
eurjchem-1080	43	3	solution	solution	NOUN
eurjchem-1080	43	4	was	be	AUX
eurjchem-1080	43	5	protected	protect	VERB
eurjchem-1080	43	6	from	from	ADP
eurjchem-1080	43	7	light	light	NOUN
eurjchem-1080	43	8	using	use	VERB
eurjchem-1080	43	9	aluminum	aluminum	NOUN
eurjchem-1080	43	10	foil	foil	NOUN
eurjchem-1080	43	11	and	and	CCONJ
eurjchem-1080	43	12	stored	store	VERB
eurjchem-1080	43	13	for	for	ADP
eurjchem-1080	43	14	1	1	NUM
eurjchem-1080	43	15	week	week	NOUN
eurjchem-1080	43	16	at	at	ADP
eurjchem-1080	43	17	4	4	NUM
eurjchem-1080	43	18	°	°	NOUN
eurjchem-1080	43	19	c	c	NOUN
eurjchem-1080	43	20	,	,	PUNCT
eurjchem-1080	43	21	and	and	CCONJ
eurjchem-1080	43	22	was	be	AUX
eurjchem-1080	43	23	found	find	VERB
eurjchem-1080	43	24	to	to	PART
eurjchem-1080	43	25	be	be	AUX
eurjchem-1080	43	26	stable	stable	ADJ
eurjchem-1080	43	27	during	during	ADP
eurjchem-1080	43	28	this	this	DET
eurjchem-1080	43	29	period	period	NOUN
eurjchem-1080	43	30	.	.	PUNCT
eurjchem-1080	44	1	in	in	ADP
eurjchem-1080	44	2	the	the	DET
eurjchem-1080	44	3	hplc	hplc	NOUN
eurjchem-1080	44	4	assay	assay	VERB
eurjchem-1080	44	5	,	,	PUNCT
eurjchem-1080	44	6	aliquots	aliquot	NOUN
eurjchem-1080	44	7	of	of	ADP
eurjchem-1080	44	8	the	the	DET
eurjchem-1080	44	9	standard	standard	ADJ
eurjchem-1080	44	10	stock	stock	NOUN
eurjchem-1080	44	11	solution	solution	NOUN
eurjchem-1080	44	12	of	of	ADP
eurjchem-1080	44	13	sitagliptin	sitagliptin	NOUN
eurjchem-1080	44	14	phosphate	phosphate	NOUN
eurjchem-1080	44	15	were	be	AUX
eurjchem-1080	44	16	transferred	transfer	VERB
eurjchem-1080	44	17	using	use	VERB
eurjchem-1080	44	18	grade	grade	NOUN
eurjchem-1080	44	19	bulb	bulb	NOUN
eurjchem-1080	44	20	pipettes	pipette	NOUN
eurjchem-1080	44	21	into	into	ADP
eurjchem-1080	44	22	10	10	NUM
eurjchem-1080	44	23	ml	ml	NOUN
eurjchem-1080	44	24	volumetric	volumetric	ADJ
eurjchem-1080	44	25	flasks	flask	NOUN
eurjchem-1080	44	26	.	.	PUNCT
eurjchem-1080	45	1	the	the	DET
eurjchem-1080	45	2	solutions	solution	NOUN
eurjchem-1080	45	3	were	be	AUX
eurjchem-1080	45	4	made	make	VERB
eurjchem-1080	45	5	up	up	ADP
eurjchem-1080	45	6	to	to	PART
eurjchem-1080	45	7	volume	volume	NOUN
eurjchem-1080	45	8	with	with	ADP
eurjchem-1080	45	9	methanol	methanol	NOUN
eurjchem-1080	45	10	to	to	PART
eurjchem-1080	45	11	give	give	VERB
eurjchem-1080	45	12	final	final	ADJ
eurjchem-1080	45	13	concentrations	concentration	NOUN
eurjchem-1080	45	14	of	of	ADP
eurjchem-1080	45	15	100	100	NUM
eurjchem-1080	45	16	,	,	PUNCT
eurjchem-1080	45	17	150	150	NUM
eurjchem-1080	45	18	,	,	PUNCT
eurjchem-1080	45	19	200	200	NUM
eurjchem-1080	45	20	,	,	PUNCT
eurjchem-1080	45	21	300	300	NUM
eurjchem-1080	45	22	,	,	PUNCT
eurjchem-1080	45	23	500	500	NUM
eurjchem-1080	45	24	,	,	PUNCT
eurjchem-1080	45	25	800	800	NUM
eurjchem-1080	45	26	and	and	CCONJ
eurjchem-1080	45	27	1000	1000	NUM
eurjchem-1080	45	28	µg	µg	NOUN
eurjchem-1080	45	29	/	/	SYM
eurjchem-1080	45	30	ml	ml	NOUN
eurjchem-1080	45	31	,	,	PUNCT
eurjchem-1080	45	32	using	use	VERB
eurjchem-1080	45	33	external	external	ADJ
eurjchem-1080	45	34	standard	standard	NOUN
eurjchem-1080	45	35	(	(	PUNCT
eurjchem-1080	45	36	1000	1000	NUM
eurjchem-1080	45	37	µg	µg	NOUN
eurjchem-1080	45	38	/	/	SYM
eurjchem-1080	45	39	ml	ml	NOUN
eurjchem-1080	45	40	)	)	PUNCT
eurjchem-1080	45	41	.	.	PUNCT
eurjchem-1080	46	1	2.5	2.5	NUM
eurjchem-1080	46	2	.	.	PUNCT
eurjchem-1080	47	1	preparation	preparation	NOUN
eurjchem-1080	47	2	of	of	ADP
eurjchem-1080	47	3	tablets	tablet	NOUN
eurjchem-1080	47	4	for	for	ADP
eurjchem-1080	47	5	assay	assay	ADJ
eurjchem-1080	47	6	ten	ten	NUM
eurjchem-1080	47	7	tablets	tablet	NOUN
eurjchem-1080	47	8	were	be	AUX
eurjchem-1080	47	9	weighed	weigh	VERB
eurjchem-1080	47	10	and	and	CCONJ
eurjchem-1080	47	11	ground	ground	VERB
eurjchem-1080	47	12	to	to	ADP
eurjchem-1080	47	13	a	a	DET
eurjchem-1080	47	14	fine	fine	ADJ
eurjchem-1080	47	15	powder	powder	NOUN
eurjchem-1080	47	16	.	.	PUNCT
eurjchem-1080	48	1	a	a	DET
eurjchem-1080	48	2	portion	portion	NOUN
eurjchem-1080	48	3	of	of	ADP
eurjchem-1080	48	4	the	the	DET
eurjchem-1080	48	5	powdered	powdered	ADJ
eurjchem-1080	48	6	tablets	tablet	NOUN
eurjchem-1080	48	7	equivalent	equivalent	ADJ
eurjchem-1080	48	8	to	to	ADP
eurjchem-1080	48	9	100	100	NUM
eurjchem-1080	48	10	mg	mg	NOUN
eurjchem-1080	48	11	was	be	AUX
eurjchem-1080	48	12	accurately	accurately	ADV
eurjchem-1080	48	13	weighed	weigh	VERB
eurjchem-1080	48	14	into	into	ADP
eurjchem-1080	48	15	100	100	NUM
eurjchem-1080	48	16	ml‐a	ml‐a	PROPN
eurjchem-1080	48	17	grade	grade	NOUN
eurjchem-1080	48	18	volumetric	volumetric	NOUN
eurjchem-1080	48	19	flask	flask	NOUN
eurjchem-1080	48	20	and	and	CCONJ
eurjchem-1080	48	21	30	30	NUM
eurjchem-1080	48	22	ml	ml	NOUN
eurjchem-1080	48	23	methanol	methanol	NOUN
eurjchem-1080	48	24	was	be	AUX
eurjchem-1080	48	25	added	add	VERB
eurjchem-1080	48	26	.	.	PUNCT
eurjchem-1080	49	1	the	the	DET
eurjchem-1080	49	2	volumetric	volumetric	ADJ
eurjchem-1080	49	3	flask	flask	NOUN
eurjchem-1080	49	4	was	be	AUX
eurjchem-1080	49	5	sonicated	sonicate	VERB
eurjchem-1080	49	6	for	for	ADP
eurjchem-1080	49	7	20	20	NUM
eurjchem-1080	49	8	min	min	NOUN
eurjchem-1080	49	9	to	to	PART
eurjchem-1080	49	10	ensure	ensure	VERB
eurjchem-1080	49	11	complete	complete	ADJ
eurjchem-1080	49	12	dissolution	dissolution	NOUN
eurjchem-1080	49	13	of	of	ADP
eurjchem-1080	49	14	the	the	DET
eurjchem-1080	49	15	sitagliptin	sitagliptin	NOUN
eurjchem-1080	49	16	phosphate	phosphate	NOUN
eurjchem-1080	49	17	then	then	ADV
eurjchem-1080	49	18	the	the	DET
eurjchem-1080	49	19	solution	solution	NOUN
eurjchem-1080	49	20	was	be	AUX
eurjchem-1080	49	21	made	make	VERB
eurjchem-1080	49	22	up	up	ADP
eurjchem-1080	49	23	to	to	ADP
eurjchem-1080	49	24	the	the	DET
eurjchem-1080	49	25	volume	volume	NOUN
eurjchem-1080	49	26	with	with	ADP
eurjchem-1080	49	27	methanol	methanol	NOUN
eurjchem-1080	49	28	.	.	PUNCT
eurjchem-1080	50	1	suitable	suitable	ADJ
eurjchem-1080	50	2	aliquots	aliquot	NOUN
eurjchem-1080	50	3	of	of	ADP
eurjchem-1080	50	4	solution	solution	NOUN
eurjchem-1080	50	5	were	be	AUX
eurjchem-1080	50	6	filtered	filter	VERB
eurjchem-1080	50	7	through	through	ADP
eurjchem-1080	50	8	a	a	DET
eurjchem-1080	50	9	0.45	0.45	NUM
eurjchem-1080	50	10	µm	µm	ADP
eurjchem-1080	50	11	nylon	nylon	NOUN
eurjchem-1080	50	12	filter	filter	NOUN
eurjchem-1080	50	13	and	and	CCONJ
eurjchem-1080	50	14	completed	complete	VERB
eurjchem-1080	50	15	as	as	ADP
eurjchem-1080	50	16	previously	previously	ADV
eurjchem-1080	50	17	mentioned	mention	VERB
eurjchem-1080	50	18	under	under	ADP
eurjchem-1080	50	19	preparation	preparation	NOUN
eurjchem-1080	50	20	of	of	ADP
eurjchem-1080	50	21	stock	stock	NOUN
eurjchem-1080	50	22	and	and	CCONJ
eurjchem-1080	50	23	standard	standard	ADJ
eurjchem-1080	50	24	solution	solution	NOUN
eurjchem-1080	50	25	for	for	ADP
eurjchem-1080	50	26	hplc	hplc	NOUN
eurjchem-1080	50	27	.	.	PUNCT
eurjchem-1080	51	1	2.6	2.6	NUM
eurjchem-1080	51	2	.	.	PUNCT
eurjchem-1080	51	3	forced	force	VERB
eurjchem-1080	51	4	degradation	degradation	NOUN
eurjchem-1080	51	5	studies	study	NOUN
eurjchem-1080	51	6	of	of	ADP
eurjchem-1080	51	7	authentic	authentic	ADJ
eurjchem-1080	51	8	sitagliptin	sitagliptin	NOUN
eurjchem-1080	51	9	phosphate	phosphate	NOUN
eurjchem-1080	51	10	and	and	CCONJ
eurjchem-1080	51	11	its	its	PRON
eurjchem-1080	51	12	tablet	tablet	NOUN
eurjchem-1080	51	13	formulation	formulation	NOUN
eurjchem-1080	51	14	in	in	ADP
eurjchem-1080	51	15	order	order	NOUN
eurjchem-1080	51	16	to	to	PART
eurjchem-1080	51	17	determine	determine	VERB
eurjchem-1080	51	18	whether	whether	SCONJ
eurjchem-1080	51	19	the	the	DET
eurjchem-1080	51	20	proposed	propose	VERB
eurjchem-1080	51	21	analytic	analytic	ADJ
eurjchem-1080	51	22	method	method	NOUN
eurjchem-1080	51	23	is	be	AUX
eurjchem-1080	51	24	stability‐indicating	stability‐indicate	VERB
eurjchem-1080	51	25	,	,	PUNCT
eurjchem-1080	51	26	sitagliptin	sitagliptin	NOUN
eurjchem-1080	51	27	phosphate	phosphate	NOUN
eurjchem-1080	51	28	in	in	ADP
eurjchem-1080	51	29	its	its	PRON
eurjchem-1080	51	30	tablets	tablet	NOUN
eurjchem-1080	51	31	pharmaceutical	pharmaceutical	ADJ
eurjchem-1080	51	32	dosage	dosage	NOUN
eurjchem-1080	51	33	form	form	NOUN
eurjchem-1080	51	34	and	and	CCONJ
eurjchem-1080	51	35	powder	powder	NOUN
eurjchem-1080	51	36	was	be	AUX
eurjchem-1080	51	37	stressed	stress	VERB
eurjchem-1080	51	38	under	under	ADP
eurjchem-1080	51	39	various	various	ADJ
eurjchem-1080	51	40	conditions	condition	NOUN
eurjchem-1080	51	41	to	to	PART
eurjchem-1080	51	42	conduct	conduct	VERB
eurjchem-1080	51	43	forced	forced	ADJ
eurjchem-1080	51	44	degradation	degradation	NOUN
eurjchem-1080	51	45	studies	study	NOUN
eurjchem-1080	51	46	.	.	PUNCT
eurjchem-1080	52	1	regulatory	regulatory	ADJ
eurjchem-1080	52	2	guidance	guidance	NOUN
eurjchem-1080	52	3	in	in	ADP
eurjchem-1080	52	4	ich	ich	PROPN
eurjchem-1080	52	5	,	,	PUNCT
eurjchem-1080	52	6	q2a	q2a	PROPN
eurjchem-1080	52	7	,	,	PUNCT
eurjchem-1080	52	8	q2b	q2b	PROPN
eurjchem-1080	52	9	,	,	PUNCT
eurjchem-1080	52	10	q3b	q3b	PROPN
eurjchem-1080	52	11	and	and	CCONJ
eurjchem-1080	52	12	fda	fda	PROPN
eurjchem-1080	52	13	21	21	NUM
eurjchem-1080	52	14	cfr	cfr	PROPN
eurjchem-1080	52	15	section	section	NOUN
eurjchem-1080	52	16	211	211	NUM
eurjchem-1080	52	17	require	require	VERB
eurjchem-1080	52	18	the	the	DET
eurjchem-1080	52	19	development	development	NOUN
eurjchem-1080	52	20	and	and	CCONJ
eurjchem-1080	52	21	validations	validation	NOUN
eurjchem-1080	52	22	of	of	ADP
eurjchem-1080	52	23	stability	stability	NOUN
eurjchem-1080	52	24	indicating	indicate	VERB
eurjchem-1080	52	25	potency	potency	NOUN
eurjchem-1080	52	26	assays	assay	NOUN
eurjchem-1080	52	27	[	[	X
eurjchem-1080	52	28	15	15	NUM
eurjchem-1080	52	29	]	]	PUNCT
eurjchem-1080	52	30	.	.	PUNCT
eurjchem-1080	53	1	2.6.1	2.6.1	X
eurjchem-1080	53	2	.	.	PUNCT
eurjchem-1080	53	3	oxidation	oxidation	NOUN
eurjchem-1080	53	4	solutions	solution	NOUN
eurjchem-1080	53	5	for	for	ADP
eurjchem-1080	53	6	oxidation	oxidation	NOUN
eurjchem-1080	53	7	studies	study	NOUN
eurjchem-1080	53	8	were	be	AUX
eurjchem-1080	53	9	prepared	prepare	VERB
eurjchem-1080	53	10	by	by	ADP
eurjchem-1080	53	11	dissolving	dissolve	VERB
eurjchem-1080	53	12	100	100	NUM
eurjchem-1080	53	13	mg	mg	NOUN
eurjchem-1080	53	14	of	of	ADP
eurjchem-1080	53	15	standard	standard	ADJ
eurjchem-1080	53	16	sitagliptin	sitagliptin	NOUN
eurjchem-1080	53	17	phosphate	phosphate	NOUN
eurjchem-1080	53	18	and	and	CCONJ
eurjchem-1080	53	19	powdered	powdered	ADJ
eurjchem-1080	53	20	tablets	tablet	NOUN
eurjchem-1080	53	21	containing	contain	VERB
eurjchem-1080	53	22	an	an	DET
eurjchem-1080	53	23	equivalent	equivalent	NOUN
eurjchem-1080	53	24	to	to	ADP
eurjchem-1080	53	25	100	100	NUM
eurjchem-1080	53	26	mg	mg	NOUN
eurjchem-1080	53	27	of	of	ADP
eurjchem-1080	53	28	sitagliptin	sitagliptin	NOUN
eurjchem-1080	53	29	phosphate	phosphate	NOUN
eurjchem-1080	53	30	in	in	ADP
eurjchem-1080	53	31	methanol	methanol	NOUN
eurjchem-1080	53	32	and	and	CCONJ
eurjchem-1080	53	33	3	3	NUM
eurjchem-1080	53	34	%	%	NOUN
eurjchem-1080	53	35	h2o2	h2o2	NOUN
eurjchem-1080	53	36	(	(	PUNCT
eurjchem-1080	53	37	20:80	20:80	NUM
eurjchem-1080	53	38	%	%	NOUN
eurjchem-1080	53	39	;	;	PUNCT
eurjchem-1080	53	40	v	v	NOUN
eurjchem-1080	53	41	:	:	PUNCT
eurjchem-1080	53	42	v	v	NOUN
eurjchem-1080	53	43	:)	:)	NOUN
eurjchem-1080	53	44	,	,	PUNCT
eurjchem-1080	53	45	protected	protect	VERB
eurjchem-1080	53	46	from	from	ADP
eurjchem-1080	53	47	light	light	NOUN
eurjchem-1080	53	48	and	and	CCONJ
eurjchem-1080	53	49	stored	store	VERB
eurjchem-1080	53	50	at	at	ADP
eurjchem-1080	53	51	room	room	NOUN
eurjchem-1080	53	52	temperature	temperature	NOUN
eurjchem-1080	53	53	for	for	ADP
eurjchem-1080	53	54	3	3	NUM
eurjchem-1080	53	55	days	day	NOUN
eurjchem-1080	53	56	.	.	PUNCT
eurjchem-1080	54	1	2.6.2	2.6.2	X
eurjchem-1080	54	2	.	.	PUNCT
eurjchem-1080	54	3	acid	acid	NOUN
eurjchem-1080	54	4	degradation	degradation	NOUN
eurjchem-1080	54	5	studies	study	NOUN
eurjchem-1080	54	6	solutions	solution	NOUN
eurjchem-1080	54	7	for	for	ADP
eurjchem-1080	54	8	acid	acid	NOUN
eurjchem-1080	54	9	degradation	degradation	NOUN
eurjchem-1080	54	10	studies	study	NOUN
eurjchem-1080	54	11	were	be	AUX
eurjchem-1080	54	12	achieved	achieve	VERB
eurjchem-1080	54	13	by	by	ADP
eurjchem-1080	54	14	refluxing	refluxe	VERB
eurjchem-1080	54	15	100	100	NUM
eurjchem-1080	54	16	mg	mg	ADP
eurjchem-1080	54	17	of	of	ADP
eurjchem-1080	54	18	standard	standard	ADJ
eurjchem-1080	54	19	sitagliptin	sitagliptin	NOUN
eurjchem-1080	54	20	phosphate	phosphate	NOUN
eurjchem-1080	54	21	and	and	CCONJ
eurjchem-1080	54	22	powdered	powdered	ADJ
eurjchem-1080	54	23	tablets	tablet	NOUN
eurjchem-1080	54	24	containing	contain	VERB
eurjchem-1080	54	25	an	an	DET
eurjchem-1080	54	26	equivalent	equivalent	NOUN
eurjchem-1080	54	27	to	to	ADP
eurjchem-1080	54	28	100	100	NUM
eurjchem-1080	54	29	mg	mg	NOUN
eurjchem-1080	54	30	of	of	ADP
eurjchem-1080	54	31	sitagliptin	sitagliptin	NOUN
eurjchem-1080	54	32	phosphate	phosphate	NOUN
eurjchem-1080	54	33	in	in	ADP
eurjchem-1080	54	34	2	2	NUM
eurjchem-1080	54	35	m	m	NOUN
eurjchem-1080	54	36	hydrochloric	hydrochloric	ADJ
eurjchem-1080	54	37	acid	acid	NOUN
eurjchem-1080	54	38	at	at	ADP
eurjchem-1080	54	39	100	100	NUM
eurjchem-1080	54	40	°	°	ADP
eurjchem-1080	54	41	c	c	NOUN
eurjchem-1080	54	42	in	in	ADP
eurjchem-1080	54	43	an	an	DET
eurjchem-1080	54	44	oil	oil	NOUN
eurjchem-1080	54	45	bath	bath	NOUN
eurjchem-1080	54	46	for	for	ADP
eurjchem-1080	54	47	24	24	NUM
eurjchem-1080	54	48	hr	hr	NOUN
eurjchem-1080	54	49	.	.	PUNCT
eurjchem-1080	55	1	the	the	DET
eurjchem-1080	55	2	reaction	reaction	NOUN
eurjchem-1080	55	3	mixture	mixture	NOUN
eurjchem-1080	55	4	was	be	AUX
eurjchem-1080	55	5	neutralized	neutralize	VERB
eurjchem-1080	55	6	with	with	ADP
eurjchem-1080	55	7	a~2.5	a~2.5	PROPN
eurjchem-1080	55	8	m	m	PROPN
eurjchem-1080	55	9	sodium	sodium	NOUN
eurjchem-1080	55	10	hydroxide	hydroxide	NOUN
eurjchem-1080	55	11	and	and	CCONJ
eurjchem-1080	55	12	extracted	extract	VERB
eurjchem-1080	55	13	with	with	ADP
eurjchem-1080	55	14	ethyl	ethyl	PROPN
eurjchem-1080	55	15	acetate	acetate	NOUN
eurjchem-1080	55	16	,	,	PUNCT
eurjchem-1080	55	17	dried	dry	VERB
eurjchem-1080	55	18	(	(	PUNCT
eurjchem-1080	55	19	na2so4	na2so4	NOUN
eurjchem-1080	55	20	anhydrous	anhydrous	ADJ
eurjchem-1080	55	21	)	)	PUNCT
eurjchem-1080	55	22	and	and	CCONJ
eurjchem-1080	55	23	evaporated	evaporate	VERB
eurjchem-1080	55	24	under	under	ADP
eurjchem-1080	55	25	vacuum	vacuum	NOUN
eurjchem-1080	55	26	.	.	PUNCT
eurjchem-1080	56	1	the	the	DET
eurjchem-1080	56	2	residue	residue	NOUN
eurjchem-1080	56	3	was	be	AUX
eurjchem-1080	56	4	dissolved	dissolve	VERB
eurjchem-1080	56	5	in	in	ADP
eurjchem-1080	56	6	methanol	methanol	NOUN
eurjchem-1080	56	7	(	(	PUNCT
eurjchem-1080	56	8	100	100	NUM
eurjchem-1080	56	9	ml	ml	NOUN
eurjchem-1080	56	10	)	)	PUNCT
eurjchem-1080	56	11	.	.	PUNCT
eurjchem-1080	57	1	2.6.3	2.6.3	NUM
eurjchem-1080	57	2	.	.	PUNCT
eurjchem-1080	57	3	alkali	alkali	ADJ
eurjchem-1080	57	4	degradation	degradation	NOUN
eurjchem-1080	57	5	studies	study	NOUN
eurjchem-1080	57	6	solutions	solution	NOUN
eurjchem-1080	57	7	for	for	ADP
eurjchem-1080	57	8	alkali	alkali	ADJ
eurjchem-1080	57	9	degradation	degradation	NOUN
eurjchem-1080	57	10	studies	study	NOUN
eurjchem-1080	57	11	were	be	AUX
eurjchem-1080	57	12	performed	perform	VERB
eurjchem-1080	57	13	by	by	ADP
eurjchem-1080	57	14	refluxing	refluxe	VERB
eurjchem-1080	57	15	100	100	NUM
eurjchem-1080	57	16	mg	mg	PROPN
eurjchem-1080	57	17	standard	standard	ADJ
eurjchem-1080	57	18	sitagliptin	sitagliptin	NOUN
eurjchem-1080	57	19	phosphate	phosphate	NOUN
eurjchem-1080	57	20	and	and	CCONJ
eurjchem-1080	57	21	powdered	powdered	ADJ
eurjchem-1080	57	22	tablets	tablet	NOUN
eurjchem-1080	57	23	containing	contain	VERB
eurjchem-1080	57	24	an	an	DET
eurjchem-1080	57	25	equivalent	equivalent	NOUN
eurjchem-1080	57	26	to	to	ADP
eurjchem-1080	57	27	100	100	NUM
eurjchem-1080	57	28	mg	mg	NOUN
eurjchem-1080	57	29	of	of	ADP
eurjchem-1080	57	30	sitagliptin	sitagliptin	NOUN
eurjchem-1080	57	31	phosphate	phosphate	NOUN
eurjchem-1080	57	32	in	in	ADP
eurjchem-1080	57	33	1	1	NUM
eurjchem-1080	57	34	m	m	NOUN
eurjchem-1080	57	35	sodium	sodium	NOUN
eurjchem-1080	57	36	hydroxide	hydroxide	NOUN
eurjchem-1080	57	37	at	at	ADP
eurjchem-1080	57	38	100	100	NUM
eurjchem-1080	57	39	°	°	ADP
eurjchem-1080	57	40	c	c	NOUN
eurjchem-1080	57	41	in	in	ADP
eurjchem-1080	57	42	an	an	DET
eurjchem-1080	57	43	oil	oil	NOUN
eurjchem-1080	57	44	bath	bath	NOUN
eurjchem-1080	57	45	for	for	ADP
eurjchem-1080	57	46	24	24	NUM
eurjchem-1080	57	47	hr	hr	NOUN
eurjchem-1080	57	48	.	.	PUNCT
eurjchem-1080	58	1	the	the	DET
eurjchem-1080	58	2	reaction	reaction	NOUN
eurjchem-1080	58	3	mixture	mixture	NOUN
eurjchem-1080	58	4	was	be	AUX
eurjchem-1080	58	5	then	then	ADV
eurjchem-1080	58	6	diluted	dilute	VERB
eurjchem-1080	58	7	with	with	ADP
eurjchem-1080	58	8	water	water	NOUN
eurjchem-1080	58	9	and	and	CCONJ
eurjchem-1080	58	10	extracted	extract	VERB
eurjchem-1080	58	11	with	with	ADP
eurjchem-1080	58	12	ethyl	ethyl	PROPN
eurjchem-1080	58	13	acetate	acetate	NOUN
eurjchem-1080	58	14	,	,	PUNCT
eurjchem-1080	58	15	dried	dry	VERB
eurjchem-1080	58	16	(	(	PUNCT
eurjchem-1080	58	17	na2so4	na2so4	NOUN
eurjchem-1080	58	18	anhydrous	anhydrous	ADJ
eurjchem-1080	58	19	)	)	PUNCT
eurjchem-1080	58	20	and	and	CCONJ
eurjchem-1080	58	21	evaporated	evaporate	VERB
eurjchem-1080	58	22	under	under	ADP
eurjchem-1080	58	23	vacuum	vacuum	NOUN
eurjchem-1080	58	24	.	.	PUNCT
eurjchem-1080	59	1	the	the	DET
eurjchem-1080	59	2	residue	residue	NOUN
eurjchem-1080	59	3	was	be	AUX
eurjchem-1080	59	4	dissolved	dissolve	VERB
eurjchem-1080	59	5	in	in	ADP
eurjchem-1080	59	6	methanol	methanol	NOUN
eurjchem-1080	59	7	(	(	PUNCT
eurjchem-1080	59	8	100	100	NUM
eurjchem-1080	59	9	ml	ml	NOUN
eurjchem-1080	59	10	)	)	PUNCT
eurjchem-1080	59	11	.	.	PUNCT
eurjchem-1080	60	1	2.6.4	2.6.4	NUM
eurjchem-1080	60	2	.	.	PUNCT
eurjchem-1080	61	1	neutral	neutral	ADJ
eurjchem-1080	61	2	degradation	degradation	NOUN
eurjchem-1080	61	3	studies	study	NOUN
eurjchem-1080	61	4	solutions	solution	NOUN
eurjchem-1080	61	5	for	for	ADP
eurjchem-1080	61	6	neutral	neutral	ADJ
eurjchem-1080	61	7	degradation	degradation	NOUN
eurjchem-1080	61	8	studies	study	NOUN
eurjchem-1080	61	9	were	be	AUX
eurjchem-1080	61	10	prepared	prepare	VERB
eurjchem-1080	61	11	by	by	ADP
eurjchem-1080	61	12	dissolving	dissolve	VERB
eurjchem-1080	61	13	100	100	NUM
eurjchem-1080	61	14	mg	mg	PROPN
eurjchem-1080	61	15	standard	standard	ADJ
eurjchem-1080	61	16	sitagliptin	sitagliptin	NOUN
eurjchem-1080	61	17	phosphate	phosphate	NOUN
eurjchem-1080	61	18	and	and	CCONJ
eurjchem-1080	61	19	powdered	powdered	ADJ
eurjchem-1080	61	20	tablets	tablet	NOUN
eurjchem-1080	61	21	containing	contain	VERB
eurjchem-1080	61	22	an	an	DET
eurjchem-1080	61	23	equivalent	equivalent	NOUN
eurjchem-1080	61	24	to	to	ADP
eurjchem-1080	61	25	100	100	NUM
eurjchem-1080	61	26	mg	mg	NOUN
eurjchem-1080	61	27	of	of	ADP
eurjchem-1080	61	28	sitagliptin	sitagliptin	NOUN
eurjchem-1080	61	29	phosphate	phosphate	NOUN
eurjchem-1080	61	30	in	in	ADP
eurjchem-1080	61	31	methanol	methanol	NOUN
eurjchem-1080	61	32	and	and	CCONJ
eurjchem-1080	61	33	water	water	NOUN
eurjchem-1080	61	34	(	(	PUNCT
eurjchem-1080	61	35	20:80	20:80	NUM
eurjchem-1080	61	36	,	,	PUNCT
eurjchem-1080	61	37	v	v	NOUN
eurjchem-1080	61	38	:	:	PUNCT
eurjchem-1080	61	39	v	v	NOUN
eurjchem-1080	61	40	)	)	PUNCT
eurjchem-1080	61	41	,	,	PUNCT
eurjchem-1080	61	42	protected	protect	VERB
eurjchem-1080	61	43	from	from	ADP
eurjchem-1080	61	44	light	light	NOUN
eurjchem-1080	61	45	,	,	PUNCT
eurjchem-1080	61	46	and	and	CCONJ
eurjchem-1080	61	47	stored	store	VERB
eurjchem-1080	61	48	at	at	ADP
eurjchem-1080	61	49	room	room	NOUN
eurjchem-1080	61	50	temperature	temperature	NOUN
eurjchem-1080	61	51	for	for	ADP
eurjchem-1080	61	52	3	3	NUM
eurjchem-1080	61	53	days	day	NOUN
eurjchem-1080	61	54	.	.	PUNCT
eurjchem-1080	62	1	2.6.5	2.6.5	X
eurjchem-1080	62	2	.	.	PUNCT
eurjchem-1080	62	3	temperature	temperature	NOUN
eurjchem-1080	62	4	stress	stress	NOUN
eurjchem-1080	62	5	studies	study	NOUN
eurjchem-1080	62	6	standard	standard	ADJ
eurjchem-1080	62	7	sitagliptin	sitagliptin	NOUN
eurjchem-1080	62	8	phosphate	phosphate	NOUN
eurjchem-1080	62	9	and	and	CCONJ
eurjchem-1080	62	10	its	its	PRON
eurjchem-1080	62	11	powdered	powdered	ADJ
eurjchem-1080	62	12	tablets	tablet	NOUN
eurjchem-1080	62	13	were	be	AUX
eurjchem-1080	62	14	exposed	expose	VERB
eurjchem-1080	62	15	to	to	ADP
eurjchem-1080	62	16	dry	dry	ADJ
eurjchem-1080	62	17	heat	heat	NOUN
eurjchem-1080	62	18	(	(	PUNCT
eurjchem-1080	62	19	90	90	NUM
eurjchem-1080	62	20	°	°	NOUN
eurjchem-1080	62	21	c	c	NOUN
eurjchem-1080	62	22	)	)	PUNCT
eurjchem-1080	62	23	in	in	ADP
eurjchem-1080	62	24	an	an	DET
eurjchem-1080	62	25	oven	oven	NOUN
eurjchem-1080	62	26	for	for	ADP
eurjchem-1080	62	27	3	3	NUM
eurjchem-1080	62	28	days	day	NOUN
eurjchem-1080	62	29	.	.	PUNCT
eurjchem-1080	63	1	2.6.6	2.6.6	NUM
eurjchem-1080	63	2	.	.	PUNCT
eurjchem-1080	64	1	photostability	photostability	NOUN
eurjchem-1080	64	2	degradation	degradation	NOUN
eurjchem-1080	64	3	assay	assay	VERB
eurjchem-1080	64	4	bulk	bulk	ADJ
eurjchem-1080	64	5	sitagliptin	sitagliptin	NOUN
eurjchem-1080	64	6	phosphate	phosphate	NOUN
eurjchem-1080	64	7	powder	powder	NOUN
eurjchem-1080	64	8	,	,	PUNCT
eurjchem-1080	64	9	its	its	PRON
eurjchem-1080	64	10	powdered	powdered	ADJ
eurjchem-1080	64	11	tablets	tablet	NOUN
eurjchem-1080	64	12	,	,	PUNCT
eurjchem-1080	64	13	and	and	CCONJ
eurjchem-1080	64	14	their	their	PRON
eurjchem-1080	64	15	methanolic	methanolic	NOUN
eurjchem-1080	64	16	solutions	solution	NOUN
eurjchem-1080	64	17	were	be	AUX
eurjchem-1080	64	18	exposed	expose	VERB
eurjchem-1080	64	19	to	to	ADP
eurjchem-1080	64	20	light	light	NOUN
eurjchem-1080	64	21	to	to	PART
eurjchem-1080	64	22	determine	determine	VERB
eurjchem-1080	64	23	the	the	DET
eurjchem-1080	64	24	effect	effect	NOUN
eurjchem-1080	64	25	of	of	ADP
eurjchem-1080	64	26	irradiation	irradiation	NOUN
eurjchem-1080	64	27	on	on	ADP
eurjchem-1080	64	28	the	the	DET
eurjchem-1080	64	29	stability	stability	NOUN
eurjchem-1080	64	30	of	of	ADP
eurjchem-1080	64	31	sitagliptin	sitagliptin	NOUN
eurjchem-1080	64	32	phosphate	phosphate	NOUN
eurjchem-1080	64	33	in	in	ADP
eurjchem-1080	64	34	the	the	DET
eurjchem-1080	64	35	solid	solid	ADJ
eurjchem-1080	64	36	state	state	NOUN
eurjchem-1080	64	37	and	and	CCONJ
eurjchem-1080	64	38	in	in	ADP
eurjchem-1080	64	39	the	the	DET
eurjchem-1080	64	40	solution	solution	NOUN
eurjchem-1080	64	41	form	form	NOUN
eurjchem-1080	64	42	.	.	PUNCT
eurjchem-1080	65	1	approximately	approximately	ADV
eurjchem-1080	65	2	,	,	PUNCT
eurjchem-1080	65	3	100	100	NUM
eurjchem-1080	65	4	mg	mg	NOUN
eurjchem-1080	65	5	of	of	ADP
eurjchem-1080	65	6	standard	standard	ADJ
eurjchem-1080	65	7	sitagliptin	sitagliptin	NOUN
eurjchem-1080	65	8	phosphate	phosphate	NOUN
eurjchem-1080	65	9	powders	powder	NOUN
eurjchem-1080	65	10	were	be	AUX
eurjchem-1080	65	11	spread	spread	VERB
eurjchem-1080	65	12	on	on	ADP
eurjchem-1080	65	13	a	a	DET
eurjchem-1080	65	14	glass	glass	NOUN
eurjchem-1080	65	15	dish	dish	NOUN
eurjchem-1080	65	16	in	in	ADP
eurjchem-1080	65	17	a	a	DET
eurjchem-1080	65	18	layer	layer	NOUN
eurjchem-1080	65	19	that	that	PRON
eurjchem-1080	65	20	was	be	AUX
eurjchem-1080	65	21	less	less	ADJ
eurjchem-1080	65	22	than	than	ADP
eurjchem-1080	65	23	2	2	NUM
eurjchem-1080	65	24	mm	mm	NOUN
eurjchem-1080	65	25	in	in	ADP
eurjchem-1080	65	26	thickness	thickness	NOUN
eurjchem-1080	65	27	.	.	PUNCT
eurjchem-1080	66	1	solutions	solution	NOUN
eurjchem-1080	66	2	of	of	ADP
eurjchem-1080	66	3	standard	standard	ADJ
eurjchem-1080	66	4	sitagliptin	sitagliptin	NOUN
eurjchem-1080	66	5	phosphate	phosphate	NOUN
eurjchem-1080	66	6	(	(	PUNCT
eurjchem-1080	66	7	1	1	NUM
eurjchem-1080	66	8	mg	mg	NUM
eurjchem-1080	66	9	/	/	SYM
eurjchem-1080	66	10	ml	ml	NOUN
eurjchem-1080	66	11	)	)	PUNCT
eurjchem-1080	66	12	were	be	AUX
eurjchem-1080	66	13	prepared	prepare	VERB
eurjchem-1080	66	14	in	in	ADP
eurjchem-1080	66	15	methanol	methanol	NOUN
eurjchem-1080	66	16	.	.	PUNCT
eurjchem-1080	67	1	all	all	DET
eurjchem-1080	67	2	samples	sample	NOUN
eurjchem-1080	67	3	for	for	ADP
eurjchem-1080	67	4	photostability	photostability	NOUN
eurjchem-1080	67	5	testing	testing	NOUN
eurjchem-1080	67	6	were	be	AUX
eurjchem-1080	67	7	placed	place	VERB
eurjchem-1080	67	8	in	in	ADP
eurjchem-1080	67	9	a	a	DET
eurjchem-1080	67	10	light	light	ADJ
eurjchem-1080	67	11	cabinet	cabinet	NOUN
eurjchem-1080	67	12	(	(	PUNCT
eurjchem-1080	67	13	thermolab	thermolab	PROPN
eurjchem-1080	67	14	,	,	PUNCT
eurjchem-1080	67	15	india	india	PROPN
eurjchem-1080	67	16	)	)	PUNCT
eurjchem-1080	67	17	and	and	CCONJ
eurjchem-1080	67	18	exposed	expose	VERB
eurjchem-1080	67	19	to	to	ADP
eurjchem-1080	67	20	light	light	NOUN
eurjchem-1080	67	21	for	for	ADP
eurjchem-1080	67	22	40	40	NUM
eurjchem-1080	67	23	h	h	NOUN
eurjchem-1080	67	24	resulting	result	VERB
eurjchem-1080	67	25	in	in	ADP
eurjchem-1080	67	26	an	an	DET
eurjchem-1080	67	27	overall	overall	ADJ
eurjchem-1080	67	28	illumination	illumination	NOUN
eurjchem-1080	67	29	≥200	≥200	VERB
eurjchem-1080	67	30	wh	wh	NOUN
eurjchem-1080	67	31	/	/	SYM
eurjchem-1080	67	32	m2	m2	PROPN
eurjchem-1080	67	33	at	at	ADP
eurjchem-1080	67	34	25	25	NUM
eurjchem-1080	67	35	°	°	NOUN
eurjchem-1080	67	36	c	c	NOUN
eurjchem-1080	67	37	with	with	ADP
eurjchem-1080	67	38	uv‐radiation	uv‐radiation	NOUN
eurjchem-1080	67	39	at	at	ADP
eurjchem-1080	67	40	320‐400	320‐400	PROPN
eurjchem-1080	67	41	nm	nm	NOUN
eurjchem-1080	67	42	.	.	PUNCT
eurjchem-1080	68	1	control	control	NOUN
eurjchem-1080	68	2	samples	sample	NOUN
eurjchem-1080	68	3	,	,	PUNCT
eurjchem-1080	68	4	which	which	PRON
eurjchem-1080	68	5	were	be	AUX
eurjchem-1080	68	6	protected	protect	VERB
eurjchem-1080	68	7	from	from	ADP
eurjchem-1080	68	8	light	light	NOUN
eurjchem-1080	68	9	with	with	ADP
eurjchem-1080	68	10	aluminum	aluminum	NOUN
eurjchem-1080	68	11	foil	foil	NOUN
eurjchem-1080	68	12	,	,	PUNCT
eurjchem-1080	68	13	were	be	AUX
eurjchem-1080	68	14	also	also	ADV
eurjchem-1080	68	15	placed	place	VERB
eurjchem-1080	68	16	in	in	ADP
eurjchem-1080	68	17	the	the	DET
eurjchem-1080	68	18	light	light	ADJ
eurjchem-1080	68	19	cabinet	cabinet	NOUN
eurjchem-1080	68	20	and	and	CCONJ
eurjchem-1080	68	21	exposed	expose	VERB
eurjchem-1080	68	22	concurrently	concurrently	ADV
eurjchem-1080	68	23	following	follow	VERB
eurjchem-1080	68	24	the	the	DET
eurjchem-1080	68	25	removal	removal	NOUN
eurjchem-1080	68	26	from	from	ADP
eurjchem-1080	68	27	the	the	DET
eurjchem-1080	68	28	light	light	ADJ
eurjchem-1080	68	29	cabinet	cabinet	NOUN
eurjchem-1080	68	30	.	.	PUNCT
eurjchem-1080	69	1	3	3	X
eurjchem-1080	69	2	.	.	NOUN
eurjchem-1080	69	3	results	result	NOUN
eurjchem-1080	69	4	and	and	CCONJ
eurjchem-1080	69	5	discussion	discussion	NOUN
eurjchem-1080	69	6	3.1	3.1	NUM
eurjchem-1080	69	7	.	.	PUNCT
eurjchem-1080	70	1	hplc	hplc	NOUN
eurjchem-1080	70	2	method	method	NOUN
eurjchem-1080	70	3	development	development	NOUN
eurjchem-1080	70	4	and	and	CCONJ
eurjchem-1080	70	5	optimization	optimization	NOUN
eurjchem-1080	70	6	poroshell	poroshell	VERB
eurjchem-1080	70	7	120	120	NUM
eurjchem-1080	70	8	ec‐c18	ec‐c18	NOUN
eurjchem-1080	70	9	(	(	PUNCT
eurjchem-1080	70	10	100	100	NUM
eurjchem-1080	70	11	×	×	NOUN
eurjchem-1080	70	12	4.6	4.6	NUM
eurjchem-1080	70	13	mm	mm	NOUN
eurjchem-1080	70	14	,	,	PUNCT
eurjchem-1080	70	15	i.d	i.d	PROPN
eurjchem-1080	70	16	.	.	PROPN
eurjchem-1080	70	17	)	)	PUNCT
eurjchem-1080	70	18	,	,	PUNCT
eurjchem-1080	70	19	pursuit	pursuit	VERB
eurjchem-1080	70	20	5pfp	5pfp	NUM
eurjchem-1080	70	21	(	(	PUNCT
eurjchem-1080	70	22	150	150	NUM
eurjchem-1080	70	23	×	×	NOUN
eurjchem-1080	70	24	4.6	4.6	NUM
eurjchem-1080	70	25	mm	mm	NOUN
eurjchem-1080	70	26	,	,	PUNCT
eurjchem-1080	70	27	i.d	i.d	PROPN
eurjchem-1080	70	28	.	.	PROPN
eurjchem-1080	70	29	)	)	PUNCT
eurjchem-1080	70	30	and	and	CCONJ
eurjchem-1080	70	31	chromolith	chromolith	VERB
eurjchem-1080	70	32	performance	performance	NOUN
eurjchem-1080	70	33	rp‐18e	rp‐18e	VERB
eurjchem-1080	70	34	(	(	PUNCT
eurjchem-1080	70	35	100	100	NUM
eurjchem-1080	70	36	×	×	NOUN
eurjchem-1080	70	37	4.6	4.6	NUM
eurjchem-1080	70	38	mm	mm	NOUN
eurjchem-1080	70	39	)	)	PUNCT
eurjchem-1080	70	40	columns	column	NOUN
eurjchem-1080	70	41	were	be	AUX
eurjchem-1080	70	42	used	use	VERB
eurjchem-1080	70	43	for	for	ADP
eurjchem-1080	70	44	the	the	DET
eurjchem-1080	70	45	determination	determination	NOUN
eurjchem-1080	70	46	of	of	ADP
eurjchem-1080	70	47	sitagliptin	sitagliptin	NOUN
eurjchem-1080	70	48	phosphate	phosphate	NOUN
eurjchem-1080	70	49	.	.	PUNCT
eurjchem-1080	71	1	saleh	saleh	NOUN
eurjchem-1080	71	2	et	et	PROPN
eurjchem-1080	71	3	al	al	PROPN
eurjchem-1080	71	4	.	.	PUNCT
eurjchem-1080	71	5	/	/	SYM
eurjchem-1080	71	6	european	european	PROPN
eurjchem-1080	71	7	journal	journal	PROPN
eurjchem-1080	71	8	of	of	ADP
eurjchem-1080	71	9	chemistry	chemistry	NOUN
eurjchem-1080	71	10	5	5	NUM
eurjchem-1080	71	11	(	(	PUNCT
eurjchem-1080	71	12	3	3	NUM
eurjchem-1080	71	13	)	)	PUNCT
eurjchem-1080	71	14	(	(	PUNCT
eurjchem-1080	71	15	2014	2014	NUM
eurjchem-1080	71	16	)	)	PUNCT
eurjchem-1080	72	1	497‐502	497‐502	NOUN
eurjchem-1080	72	2	499	499	NUM
eurjchem-1080	72	3	table	table	NOUN
eurjchem-1080	72	4	1	1	NUM
eurjchem-1080	72	5	comparative	comparative	ADJ
eurjchem-1080	72	6	chromatographic	chromatographic	ADJ
eurjchem-1080	72	7	and	and	CCONJ
eurjchem-1080	72	8	validation	validation	NOUN
eurjchem-1080	72	9	parameters	parameter	NOUN
eurjchem-1080	72	10	of	of	ADP
eurjchem-1080	72	11	sitagliptin	sitagliptin	NOUN
eurjchem-1080	72	12	using	use	VERB
eurjchem-1080	72	13	different	different	ADJ
eurjchem-1080	72	14	stationary	stationary	ADJ
eurjchem-1080	72	15	phases	phase	NOUN
eurjchem-1080	72	16	parameter	parameter	NOUN
eurjchem-1080	72	17	poroshell	poroshell	VERB
eurjchem-1080	72	18	120	120	NUM
eurjchem-1080	72	19	ec‐c18	ec‐c18	NOUN
eurjchem-1080	72	20	column	column	NOUN
eurjchem-1080	72	21	chromolith	chromolith	NOUN
eurjchem-1080	72	22	performance	performance	NOUN
eurjchem-1080	72	23	rp‐18e	rp‐18e	PUNCT
eurjchem-1080	72	24	column	column	NOUN
eurjchem-1080	72	25	pursuit	pursuit	NOUN
eurjchem-1080	72	26	5pfp	5pfp	NUM
eurjchem-1080	72	27	column	column	NOUN
eurjchem-1080	72	28	regression	regression	NOUN
eurjchem-1080	72	29	equation	equation	NOUN
eurjchem-1080	72	30	,	,	PUNCT
eurjchem-1080	72	31	r2	r2	PROPN
eurjchem-1080	72	32	y	y	PROPN
eurjchem-1080	72	33	=	=	SYM
eurjchem-1080	72	34	0.0010x‐0.008	0.0010x‐0.008	PROPN
eurjchem-1080	72	35	,	,	PUNCT
eurjchem-1080	72	36	0.999	0.999	NUM
eurjchem-1080	72	37	y	y	NOUN
eurjchem-1080	72	38	=	=	PUNCT
eurjchem-1080	72	39	0.0010x‐0.010	0.0010x‐0.010	PROPN
eurjchem-1080	72	40	,	,	PUNCT
eurjchem-1080	72	41	0.999	0.999	NUM
eurjchem-1080	72	42	y	y	PROPN
eurjchem-1080	72	43	=	=	PUNCT
eurjchem-1080	72	44	0.0010x‐0.014	0.0010x‐0.014	PROPN
eurjchem-1080	72	45	,	,	PUNCT
eurjchem-1080	72	46	0.999	0.999	NUM
eurjchem-1080	72	47	capacity	capacity	NOUN
eurjchem-1080	72	48	factor	factor	NOUN
eurjchem-1080	72	49	(	(	PUNCT
eurjchem-1080	72	50	k	k	NOUN
eurjchem-1080	72	51	`	`	PUNCT
eurjchem-1080	72	52	)	)	PUNCT
eurjchem-1080	72	53	0.399	0.399	NUM
eurjchem-1080	72	54	0.200	0.200	NUM
eurjchem-1080	72	55	0.696	0.696	NUM
eurjchem-1080	72	56	time	time	NOUN
eurjchem-1080	72	57	of	of	ADP
eurjchem-1080	72	58	analysis	analysis	NOUN
eurjchem-1080	72	59	(	(	PUNCT
eurjchem-1080	72	60	min	min	NOUN
eurjchem-1080	72	61	)	)	PUNCT
eurjchem-1080	72	62	10.000	10.000	NUM
eurjchem-1080	72	63	10.000	10.000	NUM
eurjchem-1080	72	64	10.000	10.000	NUM
eurjchem-1080	72	65	retention	retention	NOUN
eurjchem-1080	72	66	time	time	NOUN
eurjchem-1080	72	67	(	(	PUNCT
eurjchem-1080	72	68	min	min	NOUN
eurjchem-1080	72	69	)	)	PUNCT
eurjchem-1080	72	70	2.629	2.629	NUM
eurjchem-1080	72	71	3.418	3.418	NUM
eurjchem-1080	72	72	5.713	5.713	NUM
eurjchem-1080	72	73	no	no	NOUN
eurjchem-1080	72	74	.	.	PUNCT
eurjchem-1080	72	75	of	of	ADP
eurjchem-1080	72	76	theoretical	theoretical	ADJ
eurjchem-1080	72	77	plates	plate	NOUN
eurjchem-1080	72	78	(	(	PUNCT
eurjchem-1080	72	79	n	n	CCONJ
eurjchem-1080	72	80	)	)	PUNCT
eurjchem-1080	72	81	8794.286	8794.286	PROPN
eurjchem-1080	73	1	4673.200	4673.200	NUM
eurjchem-1080	73	2	19130.824	19130.824	NUM
eurjchem-1080	73	3	no	no	NOUN
eurjchem-1080	73	4	.	.	PUNCT
eurjchem-1080	73	5	of	of	ADP
eurjchem-1080	73	6	theoretical	theoretical	ADJ
eurjchem-1080	73	7	plates	plate	NOUN
eurjchem-1080	73	8	/	/	SYM
eurjchem-1080	73	9	mm	mm	PROPN
eurjchem-1080	73	10	87.94286	87.94286	NUM
eurjchem-1080	73	11	46.73200	46.73200	NUM
eurjchem-1080	73	12	12.75388	12.75388	NUM
eurjchem-1080	73	13	tailing	tail	VERB
eurjchem-1080	73	14	factor	factor	NOUN
eurjchem-1080	73	15	2.5	2.5	NUM
eurjchem-1080	73	16	1.4	1.4	NUM
eurjchem-1080	73	17	2	2	NUM
eurjchem-1080	73	18	asymmetry	asymmetry	NOUN
eurjchem-1080	73	19	factor	factor	NOUN
eurjchem-1080	73	20	3	3	NUM
eurjchem-1080	73	21	2	2	NUM
eurjchem-1080	73	22	3	3	NUM
eurjchem-1080	73	23	linearity	linearity	NOUN
eurjchem-1080	73	24	(	(	PUNCT
eurjchem-1080	73	25	µg	µg	NOUN
eurjchem-1080	73	26	/	/	SYM
eurjchem-1080	73	27	ml	ml	NOUN
eurjchem-1080	73	28	)	)	PUNCT
eurjchem-1080	73	29	100‐1000	100‐1000	NUM
eurjchem-1080	73	30	100‐1000	100‐1000	NUM
eurjchem-1080	73	31	100‐1000	100‐1000	NUM
eurjchem-1080	73	32	sensitivity	sensitivity	NOUN
eurjchem-1080	73	33	(	(	PUNCT
eurjchem-1080	73	34	µg	µg	NOUN
eurjchem-1080	73	35	/	/	SYM
eurjchem-1080	73	36	ml	ml	NOUN
eurjchem-1080	73	37	)	)	PUNCT
eurjchem-1080	73	38	100	100	NUM
eurjchem-1080	73	39	100	100	NUM
eurjchem-1080	73	40	100	100	NUM
eurjchem-1080	73	41	precision	precision	NOUN
eurjchem-1080	73	42	repeatability	repeatability	NOUN
eurjchem-1080	73	43	(	(	PUNCT
eurjchem-1080	73	44	intraday	intraday	NOUN
eurjchem-1080	73	45	)	)	PUNCT
eurjchem-1080	73	46	1.23	1.23	NUM
eurjchem-1080	73	47	0.99	0.99	NUM
eurjchem-1080	73	48	0.62	0.62	NUM
eurjchem-1080	73	49	‐	‐	NOUN
eurjchem-1080	73	50	‐	‐	ADV
eurjchem-1080	73	51	‐	‐	ADV
eurjchem-1080	73	52	‐	‐	ADV
eurjchem-1080	73	53	‐	‐	ADP
eurjchem-1080	73	54	‐	‐	ADJ
eurjchem-1080	73	55	intermediate	intermediate	ADJ
eurjchem-1080	73	56	precision	precision	NOUN
eurjchem-1080	73	57	(	(	PUNCT
eurjchem-1080	73	58	interday	interday	PROPN
eurjchem-1080	73	59	)	)	PUNCT
eurjchem-1080	73	60	1.60	1.60	NUM
eurjchem-1080	73	61	1.20	1.20	NUM
eurjchem-1080	73	62	0.99	0.99	NUM
eurjchem-1080	73	63	‐	‐	NOUN
eurjchem-1080	73	64	‐	‐	ADV
eurjchem-1080	73	65	‐	‐	ADV
eurjchem-1080	73	66	‐	‐	ADV
eurjchem-1080	73	67	‐	‐	ADP
eurjchem-1080	73	68	‐	‐	ADJ
eurjchem-1080	73	69	accuracy	accuracy	NOUN
eurjchem-1080	73	70	1.23	1.23	NUM
eurjchem-1080	73	71	0.82	0.82	NUM
eurjchem-1080	73	72	0.63	0.63	NUM
eurjchem-1080	73	73	‐	‐	NOUN
eurjchem-1080	73	74	‐	‐	ADV
eurjchem-1080	73	75	‐	‐	ADV
eurjchem-1080	73	76	‐	‐	ADV
eurjchem-1080	73	77	‐	‐	ADV
eurjchem-1080	73	78	‐	‐	ADJ
eurjchem-1080	73	79	selectivity	selectivity	NOUN
eurjchem-1080	73	80	1.34	1.34	NUM
eurjchem-1080	73	81	1.20	1.20	NUM
eurjchem-1080	73	82	1.30	1.30	NUM
eurjchem-1080	73	83	l.o.d	l.o.d	X
eurjchem-1080	73	84	.	.	PUNCT
eurjchem-1080	74	1	(	(	PUNCT
eurjchem-1080	74	2	µg	µg	NOUN
eurjchem-1080	74	3	/	/	SYM
eurjchem-1080	74	4	ml	ml	NOUN
eurjchem-1080	74	5	)	)	PUNCT
eurjchem-1080	74	6	10	10	NUM
eurjchem-1080	74	7	‐	‐	NOUN
eurjchem-1080	74	8	‐	‐	ADV
eurjchem-1080	74	9	l.o.q	l.o.q	ADV
eurjchem-1080	74	10	.	.	PUNCT
eurjchem-1080	75	1	(	(	PUNCT
eurjchem-1080	75	2	µg	µg	NOUN
eurjchem-1080	75	3	/	/	SYM
eurjchem-1080	75	4	ml	ml	NOUN
eurjchem-1080	75	5	)	)	PUNCT
eurjchem-1080	75	6	30	30	NUM
eurjchem-1080	75	7	‐	‐	NOUN
eurjchem-1080	75	8	‐	‐	ADJ
eurjchem-1080	75	9	calibration	calibration	NOUN
eurjchem-1080	75	10	curves	curve	NOUN
eurjchem-1080	75	11	,	,	PUNCT
eurjchem-1080	75	12	correlation	correlation	NOUN
eurjchem-1080	75	13	coefficient	coefficient	NOUN
eurjchem-1080	75	14	,	,	PUNCT
eurjchem-1080	75	15	slope	slope	NOUN
eurjchem-1080	75	16	,	,	PUNCT
eurjchem-1080	75	17	intercept	intercept	NOUN
eurjchem-1080	75	18	,	,	PUNCT
eurjchem-1080	75	19	capacity	capacity	NOUN
eurjchem-1080	75	20	factor	factor	NOUN
eurjchem-1080	75	21	,	,	PUNCT
eurjchem-1080	75	22	retention	retention	NOUN
eurjchem-1080	75	23	time	time	NOUN
eurjchem-1080	75	24	,	,	PUNCT
eurjchem-1080	75	25	number	number	NOUN
eurjchem-1080	75	26	of	of	ADP
eurjchem-1080	75	27	theoretical	theoretical	ADJ
eurjchem-1080	75	28	plates	plate	NOUN
eurjchem-1080	75	29	,	,	PUNCT
eurjchem-1080	75	30	number	number	NOUN
eurjchem-1080	75	31	of	of	ADP
eurjchem-1080	75	32	theoretical	theoretical	ADJ
eurjchem-1080	75	33	plates	plate	NOUN
eurjchem-1080	75	34	/	/	SYM
eurjchem-1080	75	35	mm	mm	NOUN
eurjchem-1080	75	36	,	,	PUNCT
eurjchem-1080	75	37	tailing	tail	VERB
eurjchem-1080	75	38	factor	factor	NOUN
eurjchem-1080	75	39	and	and	CCONJ
eurjchem-1080	75	40	asymmetry	asymmetry	NOUN
eurjchem-1080	75	41	factors	factor	NOUN
eurjchem-1080	75	42	were	be	AUX
eurjchem-1080	75	43	determined	determine	VERB
eurjchem-1080	75	44	using	use	VERB
eurjchem-1080	75	45	the	the	DET
eurjchem-1080	75	46	previously	previously	ADV
eurjchem-1080	75	47	mentioned	mention	VERB
eurjchem-1080	75	48	columns	column	NOUN
eurjchem-1080	75	49	as	as	SCONJ
eurjchem-1080	75	50	shown	show	VERB
eurjchem-1080	75	51	in	in	ADP
eurjchem-1080	75	52	table	table	NOUN
eurjchem-1080	75	53	1	1	NUM
eurjchem-1080	75	54	.	.	PUNCT
eurjchem-1080	76	1	it	it	PRON
eurjchem-1080	76	2	was	be	AUX
eurjchem-1080	76	3	that	that	DET
eurjchem-1080	76	4	poroshell	poroshell	PROPN
eurjchem-1080	76	5	120	120	NUM
eurjchem-1080	76	6	ec‐c18	ec‐c18	NOUN
eurjchem-1080	76	7	has	have	AUX
eurjchem-1080	76	8	achieved	achieve	VERB
eurjchem-1080	76	9	the	the	DET
eurjchem-1080	76	10	best	good	ADJ
eurjchem-1080	76	11	separation	separation	NOUN
eurjchem-1080	76	12	due	due	ADP
eurjchem-1080	76	13	to	to	ADP
eurjchem-1080	76	14	it	it	PRON
eurjchem-1080	76	15	has	have	VERB
eurjchem-1080	76	16	the	the	DET
eurjchem-1080	76	17	highest	high	ADJ
eurjchem-1080	76	18	number	number	NOUN
eurjchem-1080	76	19	of	of	ADP
eurjchem-1080	76	20	theoretical	theoretical	ADJ
eurjchem-1080	76	21	plates	plate	NOUN
eurjchem-1080	76	22	/	/	SYM
eurjchem-1080	76	23	mm	mm	NOUN
eurjchem-1080	77	1	so	so	SCONJ
eurjchem-1080	77	2	it	it	PRON
eurjchem-1080	77	3	was	be	AUX
eurjchem-1080	77	4	chosen	choose	VERB
eurjchem-1080	77	5	to	to	PART
eurjchem-1080	77	6	study	study	VERB
eurjchem-1080	77	7	all	all	DET
eurjchem-1080	77	8	the	the	DET
eurjchem-1080	77	9	validation	validation	NOUN
eurjchem-1080	77	10	parameters	parameter	NOUN
eurjchem-1080	77	11	.	.	PUNCT
eurjchem-1080	78	1	the	the	DET
eurjchem-1080	78	2	method	method	NOUN
eurjchem-1080	78	3	was	be	AUX
eurjchem-1080	78	4	validated	validate	VERB
eurjchem-1080	78	5	for	for	ADP
eurjchem-1080	78	6	the	the	DET
eurjchem-1080	78	7	determination	determination	NOUN
eurjchem-1080	78	8	of	of	ADP
eurjchem-1080	78	9	sitagliptin	sitagliptin	NOUN
eurjchem-1080	78	10	phosphate	phosphate	NOUN
eurjchem-1080	78	11	in	in	ADP
eurjchem-1080	78	12	bulk	bulk	NOUN
eurjchem-1080	78	13	and	and	CCONJ
eurjchem-1080	78	14	in	in	ADP
eurjchem-1080	78	15	pharma‐	pharma‐	NOUN
eurjchem-1080	78	16	ceutical	ceutical	ADJ
eurjchem-1080	78	17	dosage	dosage	NOUN
eurjchem-1080	78	18	form	form	NOUN
eurjchem-1080	78	19	.	.	PUNCT
eurjchem-1080	79	1	the	the	DET
eurjchem-1080	79	2	stressed	stress	VERB
eurjchem-1080	79	3	samples	sample	NOUN
eurjchem-1080	79	4	were	be	AUX
eurjchem-1080	79	5	initially	initially	ADV
eurjchem-1080	79	6	analyzed	analyze	VERB
eurjchem-1080	79	7	using	use	VERB
eurjchem-1080	79	8	a	a	DET
eurjchem-1080	79	9	mobile	mobile	ADJ
eurjchem-1080	79	10	phase	phase	NOUN
eurjchem-1080	79	11	consisting	consist	VERB
eurjchem-1080	79	12	of	of	ADP
eurjchem-1080	79	13	methanol	methanol	NOUN
eurjchem-1080	79	14	:	:	PUNCT
eurjchem-1080	79	15	water	water	NOUN
eurjchem-1080	79	16	:	:	PUNCT
eurjchem-1080	79	17	triethylamine	triethylamine	NOUN
eurjchem-1080	79	18	:	:	PUNCT
eurjchem-1080	79	19	acetic	acetic	ADJ
eurjchem-1080	79	20	acid	acid	NOUN
eurjchem-1080	79	21	(	(	PUNCT
eurjchem-1080	79	22	60:40:0.1:0.1	60:40:0.1:0.1	NOUN
eurjchem-1080	79	23	;	;	PUNCT
eurjchem-1080	79	24	v	v	X
eurjchem-1080	79	25	:	:	PUNCT
eurjchem-1080	79	26	v	v	NOUN
eurjchem-1080	79	27	:	:	PUNCT
eurjchem-1080	79	28	v	v	ADJ
eurjchem-1080	79	29	:	:	PUNCT
eurjchem-1080	79	30	v	v	NOUN
eurjchem-1080	79	31	)	)	PUNCT
eurjchem-1080	79	32	which	which	PRON
eurjchem-1080	79	33	achieved	achieve	VERB
eurjchem-1080	79	34	better	well	ADJ
eurjchem-1080	79	35	separation	separation	NOUN
eurjchem-1080	79	36	without	without	ADP
eurjchem-1080	79	37	tailing	tail	VERB
eurjchem-1080	79	38	at	at	ADP
eurjchem-1080	79	39	a	a	DET
eurjchem-1080	79	40	flow	flow	NOUN
eurjchem-1080	79	41	rate	rate	NOUN
eurjchem-1080	79	42	of	of	ADP
eurjchem-1080	79	43	0.5	0.5	NUM
eurjchem-1080	79	44	ml/	ml/	NOUN
eurjchem-1080	79	45	min	min	PROPN
eurjchem-1080	79	46	and	and	CCONJ
eurjchem-1080	79	47	uv	uv	NOUN
eurjchem-1080	79	48	detection	detection	NOUN
eurjchem-1080	79	49	at	at	ADP
eurjchem-1080	79	50	268	268	NUM
eurjchem-1080	79	51	nm	nm	NOUN
eurjchem-1080	79	52	using	use	VERB
eurjchem-1080	79	53	1000	1000	NUM
eurjchem-1080	79	54	µg	µg	ADJ
eurjchem-1080	79	55	/	/	SYM
eurjchem-1080	79	56	ml	ml	ADV
eurjchem-1080	79	57	sitagliptin	sitagliptin	NOUN
eurjchem-1080	79	58	phosphate	phosphate	NOUN
eurjchem-1080	79	59	as	as	ADP
eurjchem-1080	79	60	an	an	DET
eurjchem-1080	79	61	external	external	ADJ
eurjchem-1080	79	62	standard	standard	NOUN
eurjchem-1080	79	63	.	.	PUNCT
eurjchem-1080	80	1	3.2	3.2	NUM
eurjchem-1080	80	2	.	.	PUNCT
eurjchem-1080	81	1	validation	validation	NOUN
eurjchem-1080	81	2	the	the	DET
eurjchem-1080	81	3	method	method	NOUN
eurjchem-1080	81	4	was	be	AUX
eurjchem-1080	81	5	validated	validate	VERB
eurjchem-1080	81	6	with	with	ADP
eurjchem-1080	81	7	respect	respect	NOUN
eurjchem-1080	81	8	to	to	ADP
eurjchem-1080	81	9	parameters	parameter	NOUN
eurjchem-1080	81	10	including	include	VERB
eurjchem-1080	81	11	linearity	linearity	NOUN
eurjchem-1080	81	12	,	,	PUNCT
eurjchem-1080	81	13	limit	limit	NOUN
eurjchem-1080	81	14	of	of	ADP
eurjchem-1080	81	15	quantitation	quantitation	NOUN
eurjchem-1080	81	16	(	(	PUNCT
eurjchem-1080	81	17	loq	loq	PROPN
eurjchem-1080	81	18	)	)	PUNCT
eurjchem-1080	81	19	,	,	PUNCT
eurjchem-1080	81	20	limit	limit	NOUN
eurjchem-1080	81	21	of	of	ADP
eurjchem-1080	81	22	detection	detection	NOUN
eurjchem-1080	81	23	(	(	PUNCT
eurjchem-1080	81	24	lod	lod	PROPN
eurjchem-1080	81	25	)	)	PUNCT
eurjchem-1080	81	26	,	,	PUNCT
eurjchem-1080	81	27	precision	precision	NOUN
eurjchem-1080	81	28	,	,	PUNCT
eurjchem-1080	81	29	accuracy	accuracy	NOUN
eurjchem-1080	81	30	,	,	PUNCT
eurjchem-1080	81	31	selectivity	selectivity	NOUN
eurjchem-1080	81	32	and	and	CCONJ
eurjchem-1080	81	33	recovery	recovery	NOUN
eurjchem-1080	81	34	using	use	VERB
eurjchem-1080	81	35	poroshell	poroshell	PROPN
eurjchem-1080	81	36	120	120	NUM
eurjchem-1080	81	37	ec‐c18	ec‐c18	NOUN
eurjchem-1080	81	38	.	.	PUNCT
eurjchem-1080	82	1	3.2.1	3.2.1	NUM
eurjchem-1080	82	2	.	.	PUNCT
eurjchem-1080	83	1	linearity	linearity	NOUN
eurjchem-1080	83	2	the	the	DET
eurjchem-1080	83	3	calibration	calibration	NOUN
eurjchem-1080	83	4	curves	curve	NOUN
eurjchem-1080	83	5	constructed	construct	VERB
eurjchem-1080	83	6	for	for	ADP
eurjchem-1080	83	7	sitagliptin	sitagliptin	NOUN
eurjchem-1080	83	8	phosphate	phosphate	NOUN
eurjchem-1080	83	9	were	be	AUX
eurjchem-1080	83	10	linear	linear	ADJ
eurjchem-1080	83	11	over	over	ADP
eurjchem-1080	83	12	the	the	DET
eurjchem-1080	83	13	concentration	concentration	NOUN
eurjchem-1080	83	14	range	range	NOUN
eurjchem-1080	83	15	100‐1000	100‐1000	NUM
eurjchem-1080	83	16	µg	µg	NOUN
eurjchem-1080	83	17	/	/	SYM
eurjchem-1080	83	18	ml	ml	NOUN
eurjchem-1080	83	19	.	.	PUNCT
eurjchem-1080	84	1	peak	peak	NOUN
eurjchem-1080	84	2	areas	area	NOUN
eurjchem-1080	84	3	of	of	ADP
eurjchem-1080	84	4	sitagliptin	sitagliptin	NOUN
eurjchem-1080	84	5	phosphate	phosphate	NOUN
eurjchem-1080	84	6	were	be	AUX
eurjchem-1080	84	7	plotted	plot	VERB
eurjchem-1080	84	8	versus	versus	ADP
eurjchem-1080	84	9	its	its	PRON
eurjchem-1080	84	10	concentration	concentration	NOUN
eurjchem-1080	84	11	and	and	CCONJ
eurjchem-1080	84	12	linear	linear	ADJ
eurjchem-1080	84	13	regression	regression	NOUN
eurjchem-1080	84	14	analysis	analysis	NOUN
eurjchem-1080	84	15	was	be	AUX
eurjchem-1080	84	16	performed	perform	VERB
eurjchem-1080	84	17	on	on	ADP
eurjchem-1080	84	18	the	the	DET
eurjchem-1080	84	19	resultant	resultant	NOUN
eurjchem-1080	84	20	curve	curve	NOUN
eurjchem-1080	84	21	.	.	PUNCT
eurjchem-1080	85	1	3.2.2	3.2.2	X
eurjchem-1080	85	2	.	.	PUNCT
eurjchem-1080	86	1	limit	limit	NOUN
eurjchem-1080	86	2	of	of	ADP
eurjchem-1080	86	3	quantitation	quantitation	NOUN
eurjchem-1080	86	4	(	(	PUNCT
eurjchem-1080	86	5	loq	loq	PROPN
eurjchem-1080	86	6	)	)	PUNCT
eurjchem-1080	86	7	and	and	CCONJ
eurjchem-1080	86	8	limit	limit	NOUN
eurjchem-1080	86	9	of	of	ADP
eurjchem-1080	86	10	detection	detection	NOUN
eurjchem-1080	86	11	(	(	PUNCT
eurjchem-1080	86	12	lod	lod	PROPN
eurjchem-1080	86	13	)	)	PUNCT
eurjchem-1080	86	14	the	the	DET
eurjchem-1080	86	15	loq	loq	PROPN
eurjchem-1080	86	16	and	and	CCONJ
eurjchem-1080	86	17	lod	lod	PROPN
eurjchem-1080	86	18	were	be	AUX
eurjchem-1080	86	19	determined	determine	VERB
eurjchem-1080	86	20	based	base	VERB
eurjchem-1080	86	21	on	on	ADP
eurjchem-1080	86	22	signal	signal	NOUN
eurjchem-1080	86	23	to	to	PART
eurjchem-1080	86	24	noise	noise	NOUN
eurjchem-1080	86	25	ratios	ratio	NOUN
eurjchem-1080	86	26	.	.	PUNCT
eurjchem-1080	87	1	the	the	DET
eurjchem-1080	87	2	loq	loq	PROPN
eurjchem-1080	87	3	was	be	AUX
eurjchem-1080	87	4	found	find	VERB
eurjchem-1080	87	5	to	to	PART
eurjchem-1080	87	6	be	be	AUX
eurjchem-1080	87	7	30	30	NUM
eurjchem-1080	87	8	µg	µg	NOUN
eurjchem-1080	87	9	/	/	SYM
eurjchem-1080	87	10	ml	ml	NOUN
eurjchem-1080	87	11	with	with	ADP
eurjchem-1080	87	12	a	a	DET
eurjchem-1080	87	13	resultant	resultant	NOUN
eurjchem-1080	87	14	%	%	NOUN
eurjchem-1080	87	15	.r.s.d	.r.s.d	NOUN
eurjchem-1080	87	16	of	of	ADP
eurjchem-1080	87	17	0.4	0.4	NUM
eurjchem-1080	87	18	%	%	NOUN
eurjchem-1080	87	19	(	(	PUNCT
eurjchem-1080	87	20	n	n	NOUN
eurjchem-1080	87	21	=	=	SYM
eurjchem-1080	87	22	5	5	NUM
eurjchem-1080	87	23	)	)	PUNCT
eurjchem-1080	87	24	,	,	PUNCT
eurjchem-1080	87	25	where	where	SCONJ
eurjchem-1080	87	26	the	the	DET
eurjchem-1080	87	27	lod	lod	PROPN
eurjchem-1080	87	28	was	be	AUX
eurjchem-1080	87	29	found	find	VERB
eurjchem-1080	87	30	to	to	PART
eurjchem-1080	87	31	be	be	AUX
eurjchem-1080	87	32	10	10	NUM
eurjchem-1080	87	33	µg	µg	NOUN
eurjchem-1080	87	34	/	/	SYM
eurjchem-1080	87	35	ml	ml	NOUN
eurjchem-1080	87	36	.	.	PUNCT
eurjchem-1080	88	1	3.2.3	3.2.3	X
eurjchem-1080	88	2	.	.	PUNCT
eurjchem-1080	88	3	precision	precision	NOUN
eurjchem-1080	88	4	precision	precision	NOUN
eurjchem-1080	88	5	of	of	ADP
eurjchem-1080	88	6	the	the	DET
eurjchem-1080	88	7	assay	assay	NOUN
eurjchem-1080	88	8	was	be	AUX
eurjchem-1080	88	9	investigated	investigate	VERB
eurjchem-1080	88	10	with	with	ADP
eurjchem-1080	88	11	respect	respect	NOUN
eurjchem-1080	88	12	to	to	ADP
eurjchem-1080	88	13	both	both	DET
eurjchem-1080	88	14	repeatability	repeatability	NOUN
eurjchem-1080	88	15	and	and	CCONJ
eurjchem-1080	88	16	reproducibility	reproducibility	NOUN
eurjchem-1080	88	17	.	.	PUNCT
eurjchem-1080	89	1	repeatability	repeatability	NOUN
eurjchem-1080	89	2	was	be	AUX
eurjchem-1080	89	3	investigated	investigate	VERB
eurjchem-1080	89	4	by	by	ADP
eurjchem-1080	89	5	injecting	inject	VERB
eurjchem-1080	89	6	nine	nine	NUM
eurjchem-1080	89	7	replicate	replicate	ADJ
eurjchem-1080	89	8	samples	sample	NOUN
eurjchem-1080	89	9	of	of	ADP
eurjchem-1080	89	10	each	each	PRON
eurjchem-1080	89	11	of	of	ADP
eurjchem-1080	89	12	the	the	DET
eurjchem-1080	89	13	200	200	NUM
eurjchem-1080	89	14	,	,	PUNCT
eurjchem-1080	89	15	400	400	NUM
eurjchem-1080	89	16	and	and	CCONJ
eurjchem-1080	89	17	600µg	600µg	NOUN
eurjchem-1080	89	18	/	/	SYM
eurjchem-1080	89	19	ml	ml	ADP
eurjchem-1080	89	20	where	where	SCONJ
eurjchem-1080	89	21	the	the	DET
eurjchem-1080	89	22	mean	mean	ADJ
eurjchem-1080	89	23	concentrations	concentration	NOUN
eurjchem-1080	89	24	were	be	AUX
eurjchem-1080	89	25	found	find	VERB
eurjchem-1080	89	26	to	to	PART
eurjchem-1080	89	27	be	be	AUX
eurjchem-1080	89	28	199.81	199.81	NUM
eurjchem-1080	89	29	,	,	PUNCT
eurjchem-1080	89	30	400.23	400.23	NUM
eurjchem-1080	89	31	and	and	CCONJ
eurjchem-1080	89	32	598.40	598.40	NUM
eurjchem-1080	89	33	with	with	ADP
eurjchem-1080	89	34	associated	associated	ADJ
eurjchem-1080	89	35	relative	relative	ADJ
eurjchem-1080	89	36	standard	standard	ADJ
eurjchem-1080	89	37	deviation	deviation	NOUN
eurjchem-1080	89	38	(	(	PUNCT
eurjchem-1080	89	39	%	%	INTJ
eurjchem-1080	89	40	r.s.d	r.s.d	NOUN
eurjchem-1080	89	41	.	.	PUNCT
eurjchem-1080	89	42	)	)	PUNCT
eurjchem-1080	90	1	values	value	NOUN
eurjchem-1080	90	2	of	of	ADP
eurjchem-1080	90	3	1.23	1.23	NUM
eurjchem-1080	90	4	,	,	PUNCT
eurjchem-1080	90	5	0.99	0.99	NUM
eurjchem-1080	90	6	and	and	CCONJ
eurjchem-1080	90	7	0.62	0.62	NUM
eurjchem-1080	90	8	,	,	PUNCT
eurjchem-1080	90	9	respectively	respectively	ADV
eurjchem-1080	90	10	.	.	PUNCT
eurjchem-1080	91	1	inter‐day	inter‐day	PROPN
eurjchem-1080	91	2	precision	precision	NOUN
eurjchem-1080	91	3	was	be	AUX
eurjchem-1080	91	4	assessed	assess	VERB
eurjchem-1080	91	5	by	by	ADP
eurjchem-1080	91	6	injecting	inject	VERB
eurjchem-1080	91	7	the	the	DET
eurjchem-1080	91	8	same	same	ADJ
eurjchem-1080	91	9	three	three	NUM
eurjchem-1080	91	10	concentrations	concentration	NOUN
eurjchem-1080	91	11	over	over	ADP
eurjchem-1080	91	12	3	3	NUM
eurjchem-1080	91	13	consecutive	consecutive	ADJ
eurjchem-1080	91	14	days	day	NOUN
eurjchem-1080	91	15	,	,	PUNCT
eurjchem-1080	91	16	resulting	result	VERB
eurjchem-1080	91	17	in	in	ADP
eurjchem-1080	91	18	mean	mean	ADJ
eurjchem-1080	91	19	concentrations	concentration	NOUN
eurjchem-1080	91	20	of	of	ADP
eurjchem-1080	91	21	sitagliptin	sitagliptin	NOUN
eurjchem-1080	91	22	phosphate	phosphate	NOUN
eurjchem-1080	91	23	of	of	ADP
eurjchem-1080	91	24	200.30	200.30	NUM
eurjchem-1080	91	25	,	,	PUNCT
eurjchem-1080	91	26	400.48	400.48	NUM
eurjchem-1080	91	27	and	and	CCONJ
eurjchem-1080	91	28	600.22	600.22	NUM
eurjchem-1080	91	29	µg	µg	NOUN
eurjchem-1080	91	30	/	/	SYM
eurjchem-1080	91	31	ml	ml	NOUN
eurjchem-1080	91	32	and	and	CCONJ
eurjchem-1080	91	33	associated	associate	VERB
eurjchem-1080	91	34	%	%	NOUN
eurjchem-1080	91	35	r.s.d	r.s.d	NOUN
eurjchem-1080	91	36	of	of	ADP
eurjchem-1080	91	37	1.60	1.60	NUM
eurjchem-1080	91	38	,	,	PUNCT
eurjchem-1080	91	39	1.20	1.20	NUM
eurjchem-1080	91	40	and	and	CCONJ
eurjchem-1080	91	41	0.99	0.99	NUM
eurjchem-1080	91	42	%	%	NOUN
eurjchem-1080	91	43	,	,	PUNCT
eurjchem-1080	91	44	respectively	respectively	ADV
eurjchem-1080	91	45	.	.	PUNCT
eurjchem-1080	92	1	3.2.4	3.2.4	NUM
eurjchem-1080	92	2	.	.	PUNCT
eurjchem-1080	92	3	accuracy	accuracy	NOUN
eurjchem-1080	92	4	accuracy	accuracy	NOUN
eurjchem-1080	92	5	of	of	ADP
eurjchem-1080	92	6	the	the	DET
eurjchem-1080	92	7	assay	assay	NOUN
eurjchem-1080	92	8	was	be	AUX
eurjchem-1080	92	9	determined	determine	VERB
eurjchem-1080	92	10	by	by	ADP
eurjchem-1080	92	11	interpolation	interpolation	NOUN
eurjchem-1080	92	12	of	of	ADP
eurjchem-1080	92	13	replicate	replicate	NOUN
eurjchem-1080	92	14	(	(	PUNCT
eurjchem-1080	92	15	n	n	NOUN
eurjchem-1080	92	16	=	=	SYM
eurjchem-1080	92	17	6	6	NUM
eurjchem-1080	92	18	)	)	PUNCT
eurjchem-1080	92	19	peak	peak	NOUN
eurjchem-1080	92	20	area	area	NOUN
eurjchem-1080	92	21	of	of	ADP
eurjchem-1080	92	22	three	three	NUM
eurjchem-1080	92	23	accuracy	accuracy	NOUN
eurjchem-1080	92	24	standards	standard	NOUN
eurjchem-1080	92	25	(	(	PUNCT
eurjchem-1080	92	26	200	200	NUM
eurjchem-1080	92	27	,	,	PUNCT
eurjchem-1080	92	28	400	400	NUM
eurjchem-1080	92	29	and	and	CCONJ
eurjchem-1080	92	30	600	600	NUM
eurjchem-1080	92	31	µg	µg	ADV
eurjchem-1080	92	32	/	/	SYM
eurjchem-1080	92	33	ml	ml	NOUN
eurjchem-1080	92	34	)	)	PUNCT
eurjchem-1080	92	35	from	from	ADP
eurjchem-1080	92	36	a	a	DET
eurjchem-1080	92	37	calibration	calibration	NOUN
eurjchem-1080	92	38	curve	curve	NOUN
eurjchem-1080	92	39	prepared	prepare	VERB
eurjchem-1080	92	40	as	as	SCONJ
eurjchem-1080	92	41	previously	previously	ADV
eurjchem-1080	92	42	described	describe	VERB
eurjchem-1080	92	43	.	.	PUNCT
eurjchem-1080	93	1	in	in	ADP
eurjchem-1080	93	2	each	each	DET
eurjchem-1080	93	3	case	case	NOUN
eurjchem-1080	93	4	the	the	DET
eurjchem-1080	93	5	percent	percent	NOUN
eurjchem-1080	93	6	relevant	relevant	ADJ
eurjchem-1080	93	7	error	error	NOUN
eurjchem-1080	93	8	was	be	AUX
eurjchem-1080	93	9	calculated	calculate	VERB
eurjchem-1080	93	10	.	.	PUNCT
eurjchem-1080	94	1	the	the	DET
eurjchem-1080	94	2	resultant	resultant	NOUN
eurjchem-1080	94	3	concentration	concentration	NOUN
eurjchem-1080	94	4	,	,	PUNCT
eurjchem-1080	94	5	were	be	AUX
eurjchem-1080	94	6	199.62±0.81	199.62±0.81	NUM
eurjchem-1080	94	7	µg	µg	ADV
eurjchem-1080	94	8	/	/	SYM
eurjchem-1080	94	9	ml	ml	NOUN
eurjchem-1080	94	10	,	,	PUNCT
eurjchem-1080	94	11	(	(	PUNCT
eurjchem-1080	94	12	mean±s.d	mean±s.d	PROPN
eurjchem-1080	94	13	.	.	PUNCT
eurjchem-1080	94	14	)	)	PUNCT
eurjchem-1080	94	15	,	,	PUNCT
eurjchem-1080	94	16	400.34±0.56	400.34±0.56	NOUN
eurjchem-1080	94	17	µg	µg	NOUN
eurjchem-1080	94	18	/	/	SYM
eurjchem-1080	94	19	ml	ml	NOUN
eurjchem-1080	94	20	and	and	CCONJ
eurjchem-1080	94	21	600.52±0.41	600.52±0.41	NUM
eurjchem-1080	94	22	µg	µg	ADV
eurjchem-1080	94	23	/	/	SYM
eurjchem-1080	94	24	ml	ml	NOUN
eurjchem-1080	94	25	with	with	ADP
eurjchem-1080	94	26	percent	percent	NOUN
eurjchem-1080	94	27	relevant	relevant	ADJ
eurjchem-1080	94	28	errors	error	NOUN
eurjchem-1080	94	29	of	of	ADP
eurjchem-1080	94	30	1.23	1.23	NUM
eurjchem-1080	94	31	,	,	PUNCT
eurjchem-1080	94	32	0.82	0.82	NUM
eurjchem-1080	94	33	and	and	CCONJ
eurjchem-1080	94	34	0.63	0.63	NUM
eurjchem-1080	94	35	,	,	PUNCT
eurjchem-1080	94	36	respectively	respectively	ADV
eurjchem-1080	94	37	.	.	PUNCT
eurjchem-1080	95	1	3.2.5	3.2.5	NUM
eurjchem-1080	95	2	.	.	PUNCT
eurjchem-1080	96	1	selectivity	selectivity	NOUN
eurjchem-1080	96	2	the	the	DET
eurjchem-1080	96	3	results	result	NOUN
eurjchem-1080	96	4	of	of	ADP
eurjchem-1080	96	5	stress	stress	NOUN
eurjchem-1080	96	6	testing	testing	NOUN
eurjchem-1080	96	7	studies	study	NOUN
eurjchem-1080	96	8	were	be	AUX
eurjchem-1080	96	9	performed	perform	VERB
eurjchem-1080	96	10	on	on	ADP
eurjchem-1080	96	11	poroshell	poroshell	PROPN
eurjchem-1080	96	12	120	120	NUM
eurjchem-1080	96	13	ec‐c18	ec‐c18	NOUN
eurjchem-1080	96	14	and	and	CCONJ
eurjchem-1080	96	15	showed	show	VERB
eurjchem-1080	96	16	a	a	DET
eurjchem-1080	96	17	high	high	ADJ
eurjchem-1080	96	18	degree	degree	NOUN
eurjchem-1080	96	19	of	of	ADP
eurjchem-1080	96	20	selectivity	selectivity	NOUN
eurjchem-1080	96	21	of	of	ADP
eurjchem-1080	96	22	this	this	DET
eurjchem-1080	96	23	method	method	NOUN
eurjchem-1080	96	24	for	for	ADP
eurjchem-1080	96	25	sitagliptin	sitagliptin	NOUN
eurjchem-1080	96	26	phosphate	phosphate	NOUN
eurjchem-1080	96	27	.	.	PUNCT
eurjchem-1080	97	1	the	the	DET
eurjchem-1080	97	2	degradation	degradation	NOUN
eurjchem-1080	97	3	of	of	ADP
eurjchem-1080	97	4	sitagliptin	sitagliptin	NOUN
eurjchem-1080	97	5	phosphate	phosphate	NOUN
eurjchem-1080	97	6	was	be	AUX
eurjchem-1080	97	7	found	find	VERB
eurjchem-1080	97	8	to	to	PART
eurjchem-1080	97	9	be	be	AUX
eurjchem-1080	97	10	similar	similar	ADJ
eurjchem-1080	97	11	for	for	ADP
eurjchem-1080	97	12	both	both	CCONJ
eurjchem-1080	97	13	the	the	DET
eurjchem-1080	97	14	tablets	tablet	NOUN
eurjchem-1080	97	15	and	and	CCONJ
eurjchem-1080	97	16	bulk	bulk	ADJ
eurjchem-1080	97	17	powder	powder	NOUN
eurjchem-1080	97	18	.	.	PUNCT
eurjchem-1080	98	1	typical	typical	ADJ
eurjchem-1080	98	2	chromatograms	chromatogram	NOUN
eurjchem-1080	98	3	obtained	obtain	VERB
eurjchem-1080	98	4	following	follow	VERB
eurjchem-1080	98	5	the	the	DET
eurjchem-1080	98	6	assay	assay	NOUN
eurjchem-1080	98	7	of	of	ADP
eurjchem-1080	98	8	pure	pure	ADJ
eurjchem-1080	98	9	bulk	bulk	ADJ
eurjchem-1080	98	10	sample	sample	NOUN
eurjchem-1080	98	11	and	and	CCONJ
eurjchem-1080	98	12	stressed	stress	VERB
eurjchem-1080	98	13	samples	sample	NOUN
eurjchem-1080	98	14	are	be	AUX
eurjchem-1080	98	15	shown	show	VERB
eurjchem-1080	98	16	in	in	ADP
eurjchem-1080	98	17	figure	figure	NOUN
eurjchem-1080	98	18	2‐4	2‐4	NUM
eurjchem-1080	98	19	.	.	PUNCT
eurjchem-1080	99	1	figure	figure	NOUN
eurjchem-1080	99	2	3	3	NUM
eurjchem-1080	99	3	showed	show	VERB
eurjchem-1080	99	4	that	that	PRON
eurjchem-1080	99	5	sitagliptin	sitagliptin	NOUN
eurjchem-1080	99	6	was	be	AUX
eurjchem-1080	99	7	completely	completely	ADV
eurjchem-1080	99	8	degraded	degrade	VERB
eurjchem-1080	99	9	by	by	ADP
eurjchem-1080	99	10	hydrogen	hydrogen	NOUN
eurjchem-1080	99	11	peroxide	peroxide	NOUN
eurjchem-1080	99	12	with	with	ADP
eurjchem-1080	99	13	the	the	DET
eurjchem-1080	99	14	appearance	appearance	NOUN
eurjchem-1080	99	15	of	of	ADP
eurjchem-1080	99	16	two	two	NUM
eurjchem-1080	99	17	degradation	degradation	NOUN
eurjchem-1080	99	18	products	product	NOUN
eurjchem-1080	99	19	at	at	ADP
eurjchem-1080	99	20	retention	retention	NOUN
eurjchem-1080	99	21	time	time	NOUN
eurjchem-1080	99	22	1.987	1.987	NUM
eurjchem-1080	99	23	and	and	CCONJ
eurjchem-1080	99	24	7.429	7.429	NUM
eurjchem-1080	99	25	min	min	NOUN
eurjchem-1080	99	26	.	.	PUNCT
eurjchem-1080	100	1	also	also	ADV
eurjchem-1080	100	2	,	,	PUNCT
eurjchem-1080	100	3	sitagliptin	sitagliptin	PROPN
eurjchem-1080	100	4	was	be	AUX
eurjchem-1080	100	5	partially	partially	ADV
eurjchem-1080	100	6	degraded	degrade	VERB
eurjchem-1080	100	7	by	by	ADP
eurjchem-1080	100	8	alkaline	alkaline	NOUN
eurjchem-1080	100	9	condition	condition	NOUN
eurjchem-1080	100	10	and	and	CCONJ
eurjchem-1080	100	11	showed	show	VERB
eurjchem-1080	100	12	three	three	NUM
eurjchem-1080	100	13	degradation	degradation	NOUN
eurjchem-1080	100	14	products	product	NOUN
eurjchem-1080	100	15	at	at	ADP
eurjchem-1080	100	16	1.921	1.921	NUM
eurjchem-1080	100	17	,	,	PUNCT
eurjchem-1080	100	18	6.535	6.535	NUM
eurjchem-1080	100	19	and	and	CCONJ
eurjchem-1080	100	20	7.430	7.430	NUM
eurjchem-1080	100	21	min	min	NOUN
eurjchem-1080	100	22	,	,	PUNCT
eurjchem-1080	100	23	while	while	SCONJ
eurjchem-1080	100	24	the	the	DET
eurjchem-1080	100	25	acidic	acidic	ADJ
eurjchem-1080	100	26	condition	condition	NOUN
eurjchem-1080	100	27	led	lead	VERB
eurjchem-1080	100	28	to	to	ADP
eurjchem-1080	100	29	partial	partial	ADJ
eurjchem-1080	100	30	degradation	degradation	NOUN
eurjchem-1080	100	31	of	of	ADP
eurjchem-1080	100	32	sitagliptin	sitagliptin	NOUN
eurjchem-1080	100	33	with	with	ADP
eurjchem-1080	100	34	the	the	DET
eurjchem-1080	100	35	formation	formation	NOUN
eurjchem-1080	100	36	of	of	ADP
eurjchem-1080	100	37	several	several	ADJ
eurjchem-1080	100	38	degradation	degradation	NOUN
eurjchem-1080	100	39	products	product	NOUN
eurjchem-1080	100	40	.	.	PUNCT
eurjchem-1080	101	1	figure	figure	NOUN
eurjchem-1080	101	2	2	2	NUM
eurjchem-1080	101	3	.	.	PUNCT
eurjchem-1080	101	4	typical	typical	ADJ
eurjchem-1080	101	5	chromatogram	chromatogram	PROPN
eurjchem-1080	101	6	of	of	ADP
eurjchem-1080	101	7	sitagliptin	sitagliptin	NOUN
eurjchem-1080	101	8	phosphate	phosphate	NOUN
eurjchem-1080	101	9	on	on	ADP
eurjchem-1080	101	10	poroshell	poroshell	PROPN
eurjchem-1080	101	11	120	120	NUM
eurjchem-1080	101	12	ec‐c18	ec‐c18	NOUN
eurjchem-1080	101	13	column	column	NOUN
eurjchem-1080	101	14	.	.	PUNCT
eurjchem-1080	102	1	500	500	NUM
eurjchem-1080	102	2	saleh	saleh	NOUN
eurjchem-1080	102	3	et	et	PROPN
eurjchem-1080	102	4	al	al	PROPN
eurjchem-1080	102	5	.	.	PUNCT
eurjchem-1080	102	6	/	/	SYM
eurjchem-1080	102	7	european	european	PROPN
eurjchem-1080	102	8	journal	journal	PROPN
eurjchem-1080	102	9	of	of	ADP
eurjchem-1080	102	10	chemistry	chemistry	NOUN
eurjchem-1080	102	11	5	5	NUM
eurjchem-1080	102	12	(	(	PUNCT
eurjchem-1080	102	13	3	3	NUM
eurjchem-1080	102	14	)	)	PUNCT
eurjchem-1080	102	15	(	(	PUNCT
eurjchem-1080	102	16	2014	2014	NUM
eurjchem-1080	102	17	)	)	PUNCT
eurjchem-1080	102	18	497‐502	497‐502	NOUN
eurjchem-1080	102	19	(	(	PUNCT
eurjchem-1080	102	20	a	a	NOUN
eurjchem-1080	102	21	)	)	PUNCT
eurjchem-1080	102	22	(	(	PUNCT
eurjchem-1080	102	23	b	b	X
eurjchem-1080	102	24	)	)	PUNCT
eurjchem-1080	102	25	(	(	PUNCT
eurjchem-1080	102	26	c	c	X
eurjchem-1080	102	27	)	)	PUNCT
eurjchem-1080	102	28	figure	figure	NOUN
eurjchem-1080	102	29	3	3	NUM
eurjchem-1080	102	30	.	.	PUNCT
eurjchem-1080	102	31	degradation	degradation	NOUN
eurjchem-1080	102	32	products	product	NOUN
eurjchem-1080	102	33	of	of	ADP
eurjchem-1080	102	34	sitagliptin	sitagliptin	NOUN
eurjchem-1080	102	35	phosphate	phosphate	NOUN
eurjchem-1080	102	36	on	on	ADP
eurjchem-1080	102	37	poroshell	poroshell	PROPN
eurjchem-1080	102	38	120	120	NUM
eurjchem-1080	102	39	ec‐c18	ec‐c18	NOUN
eurjchem-1080	102	40	column	column	NOUN
eurjchem-1080	102	41	.	.	PUNCT
eurjchem-1080	103	1	(	(	PUNCT
eurjchem-1080	103	2	a	a	X
eurjchem-1080	103	3	)	)	PUNCT
eurjchem-1080	103	4	hydrogen	hydrogen	NOUN
eurjchem-1080	103	5	peroxide	peroxide	NOUN
eurjchem-1080	103	6	degradation	degradation	NOUN
eurjchem-1080	103	7	products	product	NOUN
eurjchem-1080	103	8	,	,	PUNCT
eurjchem-1080	103	9	(	(	PUNCT
eurjchem-1080	103	10	b	b	X
eurjchem-1080	103	11	)	)	PUNCT
eurjchem-1080	103	12	alkaline	alkaline	NOUN
eurjchem-1080	103	13	degradation	degradation	NOUN
eurjchem-1080	103	14	products	product	NOUN
eurjchem-1080	103	15	,	,	PUNCT
eurjchem-1080	103	16	and	and	CCONJ
eurjchem-1080	103	17	(	(	PUNCT
eurjchem-1080	103	18	c	c	X
eurjchem-1080	103	19	)	)	PUNCT
eurjchem-1080	103	20	acidic	acidic	ADJ
eurjchem-1080	103	21	degradation	degradation	NOUN
eurjchem-1080	103	22	products	product	NOUN
eurjchem-1080	103	23	.	.	PUNCT
eurjchem-1080	104	1	figure	figure	NOUN
eurjchem-1080	104	2	4	4	NUM
eurjchem-1080	104	3	.	.	PUNCT
eurjchem-1080	104	4	lab	lab	NOUN
eurjchem-1080	104	5	mixture	mixture	NOUN
eurjchem-1080	104	6	of	of	ADP
eurjchem-1080	104	7	sitagliptine	sitagliptine	NOUN
eurjchem-1080	104	8	and	and	CCONJ
eurjchem-1080	104	9	hydrogen	hydrogen	NOUN
eurjchem-1080	104	10	peroxide	peroxide	NOUN
eurjchem-1080	104	11	degradation	degradation	NOUN
eurjchem-1080	104	12	products	product	NOUN
eurjchem-1080	104	13	on	on	ADP
eurjchem-1080	104	14	poroshell	poroshell	PROPN
eurjchem-1080	104	15	120	120	NUM
eurjchem-1080	104	16	ec‐c18	ec‐c18	NOUN
eurjchem-1080	104	17	column	column	NOUN
eurjchem-1080	104	18	.	.	PUNCT
eurjchem-1080	105	1	3.2.6	3.2.6	NUM
eurjchem-1080	105	2	.	.	PUNCT
eurjchem-1080	105	3	recovery	recovery	NOUN
eurjchem-1080	105	4	a	a	DET
eurjchem-1080	105	5	known	know	VERB
eurjchem-1080	105	6	amount	amount	NOUN
eurjchem-1080	105	7	of	of	ADP
eurjchem-1080	105	8	sitagliptin	sitagliptin	NOUN
eurjchem-1080	105	9	phosphate	phosphate	NOUN
eurjchem-1080	105	10	standard	standard	ADJ
eurjchem-1080	105	11	bulk	bulk	ADJ
eurjchem-1080	105	12	powder	powder	NOUN
eurjchem-1080	105	13	was	be	AUX
eurjchem-1080	105	14	added	add	VERB
eurjchem-1080	105	15	to	to	ADP
eurjchem-1080	105	16	aliquots	aliquot	NOUN
eurjchem-1080	105	17	(	(	PUNCT
eurjchem-1080	105	18	n	n	NOUN
eurjchem-1080	105	19	=	=	SYM
eurjchem-1080	105	20	20	20	NUM
eurjchem-1080	105	21	)	)	PUNCT
eurjchem-1080	105	22	of	of	ADP
eurjchem-1080	105	23	tablet	tablet	ADJ
eurjchem-1080	105	24	contents	content	NOUN
eurjchem-1080	105	25	,	,	PUNCT
eurjchem-1080	105	26	mixed	mixed	ADJ
eurjchem-1080	105	27	,	,	PUNCT
eurjchem-1080	105	28	and	and	CCONJ
eurjchem-1080	105	29	the	the	DET
eurjchem-1080	105	30	powder	powder	NOUN
eurjchem-1080	105	31	was	be	AUX
eurjchem-1080	105	32	extracted	extract	VERB
eurjchem-1080	105	33	and	and	CCONJ
eurjchem-1080	105	34	diluted	dilute	VERB
eurjchem-1080	105	35	to	to	PART
eurjchem-1080	105	36	yield	yield	VERB
eurjchem-1080	105	37	a	a	DET
eurjchem-1080	105	38	starting	starting	NOUN
eurjchem-1080	105	39	concentration	concentration	NOUN
eurjchem-1080	105	40	.	.	PUNCT
eurjchem-1080	106	1	this	this	DET
eurjchem-1080	106	2	solution	solution	NOUN
eurjchem-1080	106	3	was	be	AUX
eurjchem-1080	106	4	analyzed	analyze	VERB
eurjchem-1080	106	5	and	and	CCONJ
eurjchem-1080	106	6	the	the	DET
eurjchem-1080	106	7	assay	assay	NOUN
eurjchem-1080	106	8	was	be	AUX
eurjchem-1080	106	9	repeated	repeat	VERB
eurjchem-1080	106	10	(	(	PUNCT
eurjchem-1080	106	11	n	n	NOUN
eurjchem-1080	106	12	=	=	SYM
eurjchem-1080	106	13	9	9	NUM
eurjchem-1080	106	14	)	)	PUNCT
eurjchem-1080	106	15	over	over	ADP
eurjchem-1080	106	16	3	3	NUM
eurjchem-1080	106	17	consecutive	consecutive	ADJ
eurjchem-1080	106	18	days	day	NOUN
eurjchem-1080	106	19	to	to	PART
eurjchem-1080	106	20	obtain	obtain	VERB
eurjchem-1080	106	21	intermediate	intermediate	ADJ
eurjchem-1080	106	22	precision	precision	NOUN
eurjchem-1080	106	23	data	datum	NOUN
eurjchem-1080	106	24	.	.	PUNCT
eurjchem-1080	107	1	the	the	DET
eurjchem-1080	107	2	observed	observe	VERB
eurjchem-1080	107	3	concentration	concentration	NOUN
eurjchem-1080	107	4	of	of	ADP
eurjchem-1080	107	5	sitagliptin	sitagliptin	NOUN
eurjchem-1080	107	6	phosphate	phosphate	NOUN
eurjchem-1080	107	7	was	be	AUX
eurjchem-1080	107	8	found	find	VERB
eurjchem-1080	107	9	to	to	PART
eurjchem-1080	107	10	be	be	AUX
eurjchem-1080	107	11	300.00±0.42	300.00±0.42	NUM
eurjchem-1080	107	12	µg	µg	NOUN
eurjchem-1080	107	13	/	/	SYM
eurjchem-1080	107	14	ml	ml	PROPN
eurjchem-1080	107	15	(	(	PUNCT
eurjchem-1080	107	16	mean±s.d	mean±s.d	PROPN
eurjchem-1080	107	17	)	)	PUNCT
eurjchem-1080	107	18	.	.	PUNCT
eurjchem-1080	108	1	the	the	DET
eurjchem-1080	108	2	resultant	resultant	NOUN
eurjchem-1080	108	3	%	%	NOUN
eurjchem-1080	108	4	r.s.d	r.s.d	NOUN
eurjchem-1080	108	5	.	.	PUNCT
eurjchem-1080	109	1	for	for	ADP
eurjchem-1080	109	2	this	this	DET
eurjchem-1080	109	3	study	study	NOUN
eurjchem-1080	109	4	was	be	AUX
eurjchem-1080	109	5	found	find	VERB
eurjchem-1080	109	6	to	to	PART
eurjchem-1080	109	7	be	be	AUX
eurjchem-1080	109	8	0.418	0.418	NUM
eurjchem-1080	109	9	%	%	NOUN
eurjchem-1080	109	10	with	with	ADP
eurjchem-1080	109	11	a	a	DET
eurjchem-1080	109	12	corresponding	corresponding	ADJ
eurjchem-1080	109	13	percentage	percentage	NOUN
eurjchem-1080	109	14	recovery	recovery	NOUN
eurjchem-1080	109	15	value	value	NOUN
eurjchem-1080	109	16	of	of	ADP
eurjchem-1080	109	17	100.44	100.44	NUM
eurjchem-1080	109	18	%	%	NOUN
eurjchem-1080	109	19	.	.	PUNCT
eurjchem-1080	110	1	3.3	3.3	NUM
eurjchem-1080	110	2	.	.	PUNCT
eurjchem-1080	111	1	assay	assay	VERB
eurjchem-1080	111	2	the	the	DET
eurjchem-1080	111	3	proposed	propose	VERB
eurjchem-1080	111	4	method	method	NOUN
eurjchem-1080	111	5	was	be	AUX
eurjchem-1080	111	6	applied	apply	VERB
eurjchem-1080	111	7	for	for	ADP
eurjchem-1080	111	8	the	the	DET
eurjchem-1080	111	9	determination	determination	NOUN
eurjchem-1080	111	10	of	of	ADP
eurjchem-1080	111	11	sitagliptin	sitagliptin	NOUN
eurjchem-1080	111	12	phosphate	phosphate	NOUN
eurjchem-1080	111	13	in	in	ADP
eurjchem-1080	111	14	the	the	DET
eurjchem-1080	111	15	tablet	tablet	NOUN
eurjchem-1080	111	16	formulations	formulation	NOUN
eurjchem-1080	111	17	.	.	PUNCT
eurjchem-1080	112	1	the	the	DET
eurjchem-1080	112	2	results	result	NOUN
eurjchem-1080	112	3	of	of	ADP
eurjchem-1080	112	4	these	these	DET
eurjchem-1080	112	5	assays	assay	NOUN
eurjchem-1080	112	6	yielded	yield	VERB
eurjchem-1080	112	7	100.60	100.60	NUM
eurjchem-1080	112	8	%	%	NOUN
eurjchem-1080	112	9	(	(	PUNCT
eurjchem-1080	112	10	%	%	INTJ
eurjchem-1080	112	11	r.s.d	r.s.d	ADJ
eurjchem-1080	112	12	=	=	SYM
eurjchem-1080	112	13	1.62	1.62	NUM
eurjchem-1080	112	14	%	%	NOUN
eurjchem-1080	112	15	)	)	PUNCT
eurjchem-1080	112	16	of	of	ADP
eurjchem-1080	112	17	expected	expect	VERB
eurjchem-1080	112	18	amount	amount	NOUN
eurjchem-1080	112	19	of	of	ADP
eurjchem-1080	112	20	the	the	DET
eurjchem-1080	112	21	tablets	tablet	NOUN
eurjchem-1080	112	22	.	.	PUNCT
eurjchem-1080	113	1	these	these	DET
eurjchem-1080	113	2	results	result	NOUN
eurjchem-1080	113	3	indicated	indicate	VERB
eurjchem-1080	113	4	that	that	SCONJ
eurjchem-1080	113	5	the	the	DET
eurjchem-1080	113	6	method	method	NOUN
eurjchem-1080	113	7	is	be	AUX
eurjchem-1080	113	8	selective	selective	ADJ
eurjchem-1080	113	9	for	for	ADP
eurjchem-1080	113	10	the	the	DET
eurjchem-1080	113	11	assay	assay	NOUN
eurjchem-1080	113	12	of	of	ADP
eurjchem-1080	113	13	sitagliptin	sitagliptin	NOUN
eurjchem-1080	113	14	phosphates	phosphate	NOUN
eurjchem-1080	113	15	without	without	ADP
eurjchem-1080	113	16	interference	interference	NOUN
eurjchem-1080	113	17	the	the	DET
eurjchem-1080	113	18	excipient	excipient	NOUN
eurjchem-1080	113	19	used	use	VERB
eurjchem-1080	113	20	in	in	ADP
eurjchem-1080	113	21	those	those	DET
eurjchem-1080	113	22	dosage	dosage	NOUN
eurjchem-1080	113	23	forms	form	NOUN
eurjchem-1080	113	24	.	.	PUNCT
eurjchem-1080	114	1	3.4	3.4	NUM
eurjchem-1080	114	2	.	.	PUNCT
eurjchem-1080	115	1	stability	stability	NOUN
eurjchem-1080	115	2	studies	study	NOUN
eurjchem-1080	115	3	all	all	PRON
eurjchem-1080	115	4	stressed	stress	VERB
eurjchem-1080	115	5	samples	sample	NOUN
eurjchem-1080	115	6	in	in	ADP
eurjchem-1080	115	7	both	both	CCONJ
eurjchem-1080	115	8	solid	solid	ADJ
eurjchem-1080	115	9	states	state	NOUN
eurjchem-1080	115	10	and	and	CCONJ
eurjchem-1080	115	11	in	in	ADP
eurjchem-1080	115	12	solution	solution	NOUN
eurjchem-1080	115	13	forms	form	NOUN
eurjchem-1080	115	14	remained	remain	VERB
eurjchem-1080	115	15	colorless	colorless	ADJ
eurjchem-1080	115	16	.	.	PUNCT
eurjchem-1080	116	1	no	no	DET
eurjchem-1080	116	2	decomposition	decomposition	NOUN
eurjchem-1080	116	3	was	be	AUX
eurjchem-1080	116	4	observed	observe	VERB
eurjchem-1080	116	5	in	in	ADP
eurjchem-1080	116	6	neutral	neutral	ADJ
eurjchem-1080	116	7	medium	medium	NOUN
eurjchem-1080	116	8	and	and	CCONJ
eurjchem-1080	116	9	on	on	ADP
eurjchem-1080	116	10	exposure	exposure	NOUN
eurjchem-1080	116	11	of	of	ADP
eurjchem-1080	116	12	sitagliptin	sitagliptin	NOUN
eurjchem-1080	116	13	phosphate	phosphate	NOUN
eurjchem-1080	116	14	in	in	ADP
eurjchem-1080	116	15	solid	solid	ADJ
eurjchem-1080	116	16	states	state	NOUN
eurjchem-1080	116	17	and	and	CCONJ
eurjchem-1080	116	18	in	in	ADP
eurjchem-1080	116	19	solution	solution	NOUN
eurjchem-1080	116	20	forms	form	NOUN
eurjchem-1080	116	21	to	to	PART
eurjchem-1080	116	22	light	light	VERB
eurjchem-1080	116	23	in	in	ADP
eurjchem-1080	116	24	a	a	DET
eurjchem-1080	116	25	photo	photo	NOUN
eurjchem-1080	116	26	stability	stability	NOUN
eurjchem-1080	116	27	chamber	chamber	NOUN
eurjchem-1080	116	28	at	at	ADP
eurjchem-1080	116	29	room	room	NOUN
eurjchem-1080	116	30	temperature	temperature	NOUN
eurjchem-1080	116	31	.	.	PUNCT
eurjchem-1080	117	1	on	on	ADP
eurjchem-1080	117	2	the	the	DET
eurjchem-1080	117	3	other	other	ADJ
eurjchem-1080	117	4	hand	hand	NOUN
eurjchem-1080	117	5	,	,	PUNCT
eurjchem-1080	117	6	it	it	PRON
eurjchem-1080	117	7	was	be	AUX
eurjchem-1080	117	8	found	find	VERB
eurjchem-1080	117	9	that	that	SCONJ
eurjchem-1080	117	10	sitagliptin	sitagliptin	NOUN
eurjchem-1080	117	11	had	have	AUX
eurjchem-1080	117	12	been	be	AUX
eurjchem-1080	117	13	extensively	extensively	ADV
eurjchem-1080	117	14	degraded	degrade	VERB
eurjchem-1080	117	15	on	on	ADP
eurjchem-1080	117	16	treating	treat	VERB
eurjchem-1080	117	17	with	with	ADP
eurjchem-1080	117	18	3	3	NUM
eurjchem-1080	117	19	%	%	NOUN
eurjchem-1080	117	20	hydrogen	hydrogen	NOUN
eurjchem-1080	117	21	peroxide	peroxide	NOUN
eurjchem-1080	117	22	for	for	ADP
eurjchem-1080	117	23	3	3	NUM
eurjchem-1080	117	24	days	day	NOUN
eurjchem-1080	117	25	.	.	PUNCT
eurjchem-1080	118	1	the	the	DET
eurjchem-1080	118	2	retention	retention	NOUN
eurjchem-1080	118	3	time	time	NOUN
eurjchem-1080	118	4	rt	rt	PROPN
eurjchem-1080	118	5	of	of	ADP
eurjchem-1080	118	6	hydrogen	hydrogen	NOUN
eurjchem-1080	118	7	peroxide	peroxide	NOUN
eurjchem-1080	118	8	degradation	degradation	NOUN
eurjchem-1080	118	9	products	product	NOUN
eurjchem-1080	118	10	of	of	ADP
eurjchem-1080	118	11	sitagliptin	sitagliptin	NOUN
eurjchem-1080	118	12	phosphate	phosphate	NOUN
eurjchem-1080	118	13	were	be	AUX
eurjchem-1080	118	14	1.987	1.987	NUM
eurjchem-1080	118	15	and	and	CCONJ
eurjchem-1080	118	16	7.429	7.429	NUM
eurjchem-1080	118	17	min	min	NOUN
eurjchem-1080	118	18	.	.	PROPN
eurjchem-1080	118	19	also	also	ADV
eurjchem-1080	118	20	76	76	NUM
eurjchem-1080	118	21	and	and	CCONJ
eurjchem-1080	118	22	28	28	NUM
eurjchem-1080	118	23	%	%	NOUN
eurjchem-1080	118	24	degra‐	degra‐	PROPN
eurjchem-1080	118	25	dation	dation	NOUN
eurjchem-1080	118	26	was	be	AUX
eurjchem-1080	118	27	observed	observe	VERB
eurjchem-1080	118	28	in	in	ADP
eurjchem-1080	118	29	alkaline	alkaline	NOUN
eurjchem-1080	118	30	and	and	CCONJ
eurjchem-1080	118	31	acidic	acidic	ADJ
eurjchem-1080	118	32	media	medium	NOUN
eurjchem-1080	118	33	,	,	PUNCT
eurjchem-1080	118	34	respectively	respectively	ADV
eurjchem-1080	118	35	,	,	PUNCT
eurjchem-1080	118	36	as	as	SCONJ
eurjchem-1080	118	37	shown	show	VERB
eurjchem-1080	118	38	in	in	ADP
eurjchem-1080	118	39	figure	figure	NOUN
eurjchem-1080	118	40	3	3	NUM
eurjchem-1080	118	41	and	and	CCONJ
eurjchem-1080	118	42	4	4	NUM
eurjchem-1080	118	43	.	.	X
eurjchem-1080	119	1	3.4.1	3.4.1	NUM
eurjchem-1080	119	2	.	.	X
eurjchem-1080	119	3	stability‐indicating	stability‐indicate	VERB
eurjchem-1080	119	4	method	method	NOUN
eurjchem-1080	119	5	for	for	ADP
eurjchem-1080	119	6	analysis	analysis	NOUN
eurjchem-1080	119	7	of	of	ADP
eurjchem-1080	119	8	sitagliptin	sitagliptin	NOUN
eurjchem-1080	119	9	phosphate	phosphate	NOUN
eurjchem-1080	119	10	in	in	ADP
eurjchem-1080	119	11	presence	presence	NOUN
eurjchem-1080	119	12	of	of	ADP
eurjchem-1080	119	13	its	its	PRON
eurjchem-1080	119	14	hydrogen	hydrogen	NOUN
eurjchem-1080	119	15	peroxide	peroxide	NOUN
eurjchem-1080	119	16	‐oxidative	‐oxidative	ADJ
eurjchem-1080	119	17	degraded	degraded	ADJ
eurjchem-1080	119	18	products	product	NOUN
eurjchem-1080	119	19	by	by	ADP
eurjchem-1080	119	20	hplc	hplc	PROPN
eurjchem-1080	119	21	a	a	DET
eurjchem-1080	119	22	simple	simple	ADJ
eurjchem-1080	119	23	hplc	hplc	NOUN
eurjchem-1080	119	24	method	method	NOUN
eurjchem-1080	119	25	was	be	AUX
eurjchem-1080	119	26	adopted	adopt	VERB
eurjchem-1080	119	27	for	for	ADP
eurjchem-1080	119	28	the	the	DET
eurjchem-1080	119	29	simultaneous	simultaneous	ADJ
eurjchem-1080	119	30	determination	determination	NOUN
eurjchem-1080	119	31	of	of	ADP
eurjchem-1080	119	32	sitagliptin	sitagliptin	NOUN
eurjchem-1080	119	33	phosphate	phosphate	NOUN
eurjchem-1080	119	34	and	and	CCONJ
eurjchem-1080	119	35	its	its	PRON
eurjchem-1080	119	36	oxidative	oxidative	ADJ
eurjchem-1080	119	37	hydrogen	hydrogen	NOUN
eurjchem-1080	119	38	peroxide	peroxide	NOUN
eurjchem-1080	119	39	degraded	degrade	VERB
eurjchem-1080	119	40	products	product	NOUN
eurjchem-1080	119	41	in	in	ADP
eurjchem-1080	119	42	bulk	bulk	ADJ
eurjchem-1080	119	43	powder	powder	NOUN
eurjchem-1080	119	44	.	.	PUNCT
eurjchem-1080	120	1	to	to	PART
eurjchem-1080	120	2	optimize	optimize	VERB
eurjchem-1080	120	3	the	the	DET
eurjchem-1080	120	4	proposed	propose	VERB
eurjchem-1080	120	5	hplc	hplc	NOUN
eurjchem-1080	120	6	method	method	NOUN
eurjchem-1080	120	7	,	,	PUNCT
eurjchem-1080	120	8	all	all	PRON
eurjchem-1080	120	9	of	of	ADP
eurjchem-1080	120	10	the	the	DET
eurjchem-1080	120	11	experimental	experimental	ADJ
eurjchem-1080	120	12	conditions	condition	NOUN
eurjchem-1080	120	13	were	be	AUX
eurjchem-1080	120	14	investigated	investigate	VERB
eurjchem-1080	120	15	.	.	PUNCT
eurjchem-1080	121	1	to	to	PART
eurjchem-1080	121	2	optimize	optimize	VERB
eurjchem-1080	121	3	the	the	DET
eurjchem-1080	121	4	mobile	mobile	ADJ
eurjchem-1080	121	5	phases	phase	NOUN
eurjchem-1080	121	6	,	,	PUNCT
eurjchem-1080	121	7	different	different	ADJ
eurjchem-1080	121	8	systems	system	NOUN
eurjchem-1080	121	9	were	be	AUX
eurjchem-1080	121	10	tried	try	VERB
eurjchem-1080	121	11	for	for	ADP
eurjchem-1080	121	12	chromatographic	chromatographic	ADJ
eurjchem-1080	121	13	separation	separation	NOUN
eurjchem-1080	121	14	of	of	ADP
eurjchem-1080	121	15	the	the	DET
eurjchem-1080	121	16	two	two	NUM
eurjchem-1080	121	17	components	component	NOUN
eurjchem-1080	121	18	by	by	ADP
eurjchem-1080	121	19	combining	combine	VERB
eurjchem-1080	121	20	homogenous	homogenous	ADJ
eurjchem-1080	121	21	design	design	NOUN
eurjchem-1080	121	22	and	and	CCONJ
eurjchem-1080	121	23	solvent	solvent	ADJ
eurjchem-1080	121	24	polarity	polarity	NOUN
eurjchem-1080	121	25	optimization	optimization	NOUN
eurjchem-1080	121	26	.	.	PUNCT
eurjchem-1080	122	1	the	the	DET
eurjchem-1080	122	2	best	good	ADJ
eurjchem-1080	122	3	resolution	resolution	NOUN
eurjchem-1080	122	4	was	be	AUX
eurjchem-1080	122	5	achieved	achieve	VERB
eurjchem-1080	122	6	using	use	VERB
eurjchem-1080	122	7	a	a	DET
eurjchem-1080	122	8	mobile	mobile	ADJ
eurjchem-1080	122	9	phase	phase	NOUN
eurjchem-1080	122	10	consisting	consist	VERB
eurjchem-1080	122	11	of	of	ADP
eurjchem-1080	122	12	methanol	methanol	NOUN
eurjchem-1080	122	13	:	:	PUNCT
eurjchem-1080	122	14	water	water	NOUN
eurjchem-1080	122	15	:	:	PUNCT
eurjchem-1080	122	16	triethyl	triethyl	PROPN
eurjchem-1080	122	17	amine	amine	ADJ
eurjchem-1080	122	18	:	:	PUNCT
eurjchem-1080	122	19	acetic	acetic	ADJ
eurjchem-1080	122	20	acid	acid	NOUN
eurjchem-1080	122	21	(	(	PUNCT
eurjchem-1080	122	22	60:40:0.1:0.1	60:40:0.1:0.1	NOUN
eurjchem-1080	122	23	;	;	PUNCT
eurjchem-1080	122	24	v	v	X
eurjchem-1080	122	25	:	:	PUNCT
eurjchem-1080	122	26	v	v	NOUN
eurjchem-1080	122	27	:	:	PUNCT
eurjchem-1080	122	28	v	v	ADJ
eurjchem-1080	122	29	:	:	PUNCT
eurjchem-1080	122	30	v	v	NOUN
eurjchem-1080	122	31	)	)	PUNCT
eurjchem-1080	122	32	which	which	PRON
eurjchem-1080	122	33	gave	give	VERB
eurjchem-1080	122	34	good	good	ADJ
eurjchem-1080	122	35	reso‐	reso‐	PROPN
eurjchem-1080	122	36	lution	lution	PROPN
eurjchem-1080	122	37	and	and	CCONJ
eurjchem-1080	122	38	sensitivity	sensitivity	NOUN
eurjchem-1080	122	39	of	of	ADP
eurjchem-1080	122	40	all	all	DET
eurjchem-1080	122	41	components	component	NOUN
eurjchem-1080	122	42	.	.	PUNCT
eurjchem-1080	123	1	a	a	DET
eurjchem-1080	123	2	linear	linear	ADJ
eurjchem-1080	123	3	relationship	relationship	NOUN
eurjchem-1080	123	4	was	be	AUX
eurjchem-1080	123	5	obtained	obtain	VERB
eurjchem-1080	123	6	between	between	ADP
eurjchem-1080	123	7	peak	peak	NOUN
eurjchem-1080	123	8	area	area	NOUN
eurjchem-1080	123	9	and	and	CCONJ
eurjchem-1080	123	10	the	the	DET
eurjchem-1080	123	11	concentration	concentration	NOUN
eurjchem-1080	123	12	of	of	ADP
eurjchem-1080	123	13	sitagliptin	sitagliptin	NOUN
eurjchem-1080	123	14	phosphate	phosphate	NOUN
eurjchem-1080	123	15	in	in	ADP
eurjchem-1080	123	16	the	the	DET
eurjchem-1080	123	17	presence	presence	NOUN
eurjchem-1080	123	18	of	of	ADP
eurjchem-1080	123	19	its	its	PRON
eurjchem-1080	123	20	hydrogen	hydrogen	NOUN
eurjchem-1080	123	21	peroxide	peroxide	NOUN
eurjchem-1080	123	22	oxidative	oxidative	ADJ
eurjchem-1080	123	23	degraded	degraded	ADJ
eurjchem-1080	123	24	products	product	NOUN
eurjchem-1080	123	25	in	in	ADP
eurjchem-1080	123	26	the	the	DET
eurjchem-1080	123	27	range	range	NOUN
eurjchem-1080	123	28	of	of	ADP
eurjchem-1080	123	29	100‐1000	100‐1000	NUM
eurjchem-1080	123	30	µg	µg	NOUN
eurjchem-1080	123	31	/	/	SYM
eurjchem-1080	123	32	ml	ml	NOUN
eurjchem-1080	123	33	.	.	PUNCT
eurjchem-1080	124	1	the	the	DET
eurjchem-1080	124	2	linear	linear	ADJ
eurjchem-1080	124	3	regression	regression	NOUN
eurjchem-1080	124	4	equation	equation	NOUN
eurjchem-1080	124	5	was	be	AUX
eurjchem-1080	124	6	computed	compute	VERB
eurjchem-1080	124	7	as	as	ADP
eurjchem-1080	124	8	:	:	PUNCT
eurjchem-1080	124	9	y	y	PROPN
eurjchem-1080	124	10	=	=	SYM
eurjchem-1080	124	11	0.0010x+	0.0010x+	PROPN
eurjchem-1080	124	12	0.0033	0.0033	NUM
eurjchem-1080	124	13	r	r	NOUN
eurjchem-1080	124	14	=	=	SYM
eurjchem-1080	124	15	0.9998	0.9998	NUM
eurjchem-1080	124	16	(	(	PUNCT
eurjchem-1080	124	17	1	1	NUM
eurjchem-1080	124	18	)	)	PUNCT
eurjchem-1080	124	19	where	where	SCONJ
eurjchem-1080	124	20	y	y	PROPN
eurjchem-1080	124	21	is	be	AUX
eurjchem-1080	124	22	the	the	DET
eurjchem-1080	124	23	area	area	NOUN
eurjchem-1080	124	24	under	under	ADP
eurjchem-1080	124	25	the	the	DET
eurjchem-1080	124	26	peak	peak	NOUN
eurjchem-1080	124	27	,	,	PUNCT
eurjchem-1080	124	28	x	x	X
eurjchem-1080	124	29	is	be	AUX
eurjchem-1080	124	30	the	the	DET
eurjchem-1080	124	31	concentration	concentration	NOUN
eurjchem-1080	124	32	in	in	ADP
eurjchem-1080	124	33	µg	µg	ADV
eurjchem-1080	124	34	/	/	SYM
eurjchem-1080	124	35	ml	ml	NOUN
eurjchem-1080	124	36	,	,	PUNCT
eurjchem-1080	124	37	and	and	CCONJ
eurjchem-1080	124	38	r	r	NOUN
eurjchem-1080	124	39	is	be	AUX
eurjchem-1080	124	40	a	a	DET
eurjchem-1080	124	41	correlation	correlation	NOUN
eurjchem-1080	124	42	coefficient	coefficient	NOUN
eurjchem-1080	124	43	.	.	PUNCT
eurjchem-1080	125	1	the	the	DET
eurjchem-1080	125	2	results	result	NOUN
eurjchem-1080	125	3	obtained	obtain	VERB
eurjchem-1080	125	4	by	by	ADP
eurjchem-1080	125	5	applying	apply	VERB
eurjchem-1080	125	6	the	the	DET
eurjchem-1080	125	7	hplc	hplc	NOUN
eurjchem-1080	125	8	procedure	procedure	NOUN
eurjchem-1080	125	9	showed	show	VERB
eurjchem-1080	125	10	that	that	SCONJ
eurjchem-1080	125	11	sitagliptin	sitagliptin	NOUN
eurjchem-1080	125	12	phosphate	phosphate	NOUN
eurjchem-1080	125	13	can	can	AUX
eurjchem-1080	125	14	be	be	AUX
eurjchem-1080	125	15	simultaneously	simultaneously	ADV
eurjchem-1080	125	16	analyzed	analyze	VERB
eurjchem-1080	125	17	in	in	ADP
eurjchem-1080	125	18	the	the	DET
eurjchem-1080	125	19	presence	presence	NOUN
eurjchem-1080	125	20	of	of	ADP
eurjchem-1080	125	21	its	its	PRON
eurjchem-1080	125	22	hydrogen	hydrogen	NOUN
eurjchem-1080	125	23	peroxide	peroxide	NOUN
eurjchem-1080	125	24	oxidative	oxidative	NOUN
eurjchem-1080	125	25	degraded	degrade	VERB
eurjchem-1080	125	26	with	with	ADP
eurjchem-1080	125	27	mean	mean	ADJ
eurjchem-1080	125	28	recoveries	recovery	NOUN
eurjchem-1080	125	29	of	of	ADP
eurjchem-1080	125	30	100.05±1.399	100.05±1.399	NOUN
eurjchem-1080	125	31	%	%	NOUN
eurjchem-1080	125	32	,	,	PUNCT
eurjchem-1080	125	33	table	table	NOUN
eurjchem-1080	125	34	2	2	NUM
eurjchem-1080	125	35	.	.	PUNCT
eurjchem-1080	126	1	the	the	DET
eurjchem-1080	126	2	proposed	propose	VERB
eurjchem-1080	126	3	method	method	NOUN
eurjchem-1080	126	4	has	have	AUX
eurjchem-1080	126	5	been	be	AUX
eurjchem-1080	126	6	applied	apply	VERB
eurjchem-1080	126	7	to	to	ADP
eurjchem-1080	126	8	the	the	DET
eurjchem-1080	126	9	assay	assay	NOUN
eurjchem-1080	126	10	of	of	ADP
eurjchem-1080	126	11	sitagliptin	sitagliptin	NOUN
eurjchem-1080	126	12	phosphate	phosphate	NOUN
eurjchem-1080	126	13	in	in	ADP
eurjchem-1080	126	14	its	its	PRON
eurjchem-1080	126	15	tablet	tablet	NOUN
eurjchem-1080	126	16	form	form	NOUN
eurjchem-1080	126	17	without	without	ADP
eurjchem-1080	126	18	any	any	DET
eurjchem-1080	126	19	interference	interference	NOUN
eurjchem-1080	126	20	from	from	ADP
eurjchem-1080	126	21	the	the	DET
eurjchem-1080	126	22	excipients	excipient	NOUN
eurjchem-1080	126	23	.	.	PUNCT
eurjchem-1080	127	1	the	the	DET
eurjchem-1080	127	2	validity	validity	NOUN
eurjchem-1080	127	3	of	of	ADP
eurjchem-1080	127	4	the	the	DET
eurjchem-1080	127	5	suggested	suggest	VERB
eurjchem-1080	127	6	procedure	procedure	NOUN
eurjchem-1080	127	7	was	be	AUX
eurjchem-1080	127	8	further	far	ADV
eurjchem-1080	127	9	assessed	assess	VERB
eurjchem-1080	127	10	by	by	ADP
eurjchem-1080	127	11	applying	apply	VERB
eurjchem-1080	127	12	the	the	DET
eurjchem-1080	127	13	standard	standard	ADJ
eurjchem-1080	127	14	addition	addition	NOUN
eurjchem-1080	127	15	technique	technique	NOUN
eurjchem-1080	127	16	with	with	ADP
eurjchem-1080	127	17	mean	mean	ADJ
eurjchem-1080	127	18	recoveries	recovery	NOUN
eurjchem-1080	127	19	100.48±0.692	100.48±0.692	NUM
eurjchem-1080	127	20	%	%	NOUN
eurjchem-1080	127	21	,	,	PUNCT
eurjchem-1080	127	22	table	table	NOUN
eurjchem-1080	127	23	3	3	NUM
eurjchem-1080	127	24	.	.	PUNCT
eurjchem-1080	128	1	a	a	DET
eurjchem-1080	128	2	statistical	statistical	ADJ
eurjchem-1080	128	3	comparison	comparison	NOUN
eurjchem-1080	128	4	of	of	ADP
eurjchem-1080	128	5	the	the	DET
eurjchem-1080	128	6	results	result	NOUN
eurjchem-1080	128	7	obtained	obtain	VERB
eurjchem-1080	128	8	by	by	ADP
eurjchem-1080	128	9	the	the	DET
eurjchem-1080	128	10	proposed	propose	VERB
eurjchem-1080	128	11	hplc	hplc	NOUN
eurjchem-1080	128	12	method	method	NOUN
eurjchem-1080	128	13	and	and	CCONJ
eurjchem-1080	128	14	the	the	DET
eurjchem-1080	128	15	clarke	clarke	PROPN
eurjchem-1080	128	16	procedure	procedure	NOUN
eurjchem-1080	128	17	that	that	PRON
eurjchem-1080	128	18	depends	depend	VERB
eurjchem-1080	128	19	on	on	ADP
eurjchem-1080	128	20	uv	uv	NOUN
eurjchem-1080	128	21	spectrophotometric	spectrophotometric	ADJ
eurjchem-1080	128	22	determinations	determination	NOUN
eurjchem-1080	128	23	of	of	ADP
eurjchem-1080	128	24	sitagliptin	sitagliptin	NOUN
eurjchem-1080	128	25	phosphate	phosphate	NOUN
eurjchem-1080	128	26	[	[	X
eurjchem-1080	128	27	16	16	NUM
eurjchem-1080	128	28	]	]	PUNCT
eurjchem-1080	128	29	in	in	ADP
eurjchem-1080	128	30	a	a	DET
eurjchem-1080	128	31	pure	pure	ADJ
eurjchem-1080	128	32	drug	drug	NOUN
eurjchem-1080	128	33	are	be	AUX
eurjchem-1080	128	34	shown	show	VERB
eurjchem-1080	128	35	in	in	ADP
eurjchem-1080	128	36	table	table	NOUN
eurjchem-1080	128	37	4	4	NUM
eurjchem-1080	128	38	.	.	PUNCT
eurjchem-1080	129	1	the	the	DET
eurjchem-1080	129	2	calculated	calculate	VERB
eurjchem-1080	129	3	t	t	PROPN
eurjchem-1080	129	4	and	and	CCONJ
eurjchem-1080	129	5	f	f	PROPN
eurjchem-1080	129	6	values	value	NOUN
eurjchem-1080	129	7	were	be	AUX
eurjchem-1080	129	8	less	less	ADJ
eurjchem-1080	129	9	than	than	ADP
eurjchem-1080	129	10	the	the	DET
eurjchem-1080	129	11	tabulated	tabulate	VERB
eurjchem-1080	129	12	values	value	NOUN
eurjchem-1080	129	13	[	[	X
eurjchem-1080	129	14	17	17	NUM
eurjchem-1080	129	15	]	]	PUNCT
eurjchem-1080	129	16	,	,	PUNCT
eurjchem-1080	129	17	which	which	PRON
eurjchem-1080	129	18	revealed	reveal	VERB
eurjchem-1080	129	19	that	that	SCONJ
eurjchem-1080	129	20	there	there	PRON
eurjchem-1080	129	21	is	be	VERB
eurjchem-1080	129	22	no	no	DET
eurjchem-1080	129	23	significant	significant	ADJ
eurjchem-1080	129	24	difference	difference	NOUN
eurjchem-1080	129	25	with	with	ADP
eurjchem-1080	129	26	respect	respect	NOUN
eurjchem-1080	129	27	to	to	ADP
eurjchem-1080	129	28	accuracy	accuracy	NOUN
eurjchem-1080	129	29	and	and	CCONJ
eurjchem-1080	129	30	precision	precision	NOUN
eurjchem-1080	129	31	determined	determine	VERB
eurjchem-1080	129	32	through	through	ADP
eurjchem-1080	129	33	assay	assay	NOUN
eurjchem-1080	129	34	of	of	ADP
eurjchem-1080	129	35	variables	variable	NOUN
eurjchem-1080	129	36	.	.	PUNCT
eurjchem-1080	130	1	also	also	ADV
eurjchem-1080	130	2	,	,	PUNCT
eurjchem-1080	130	3	some	some	DET
eurjchem-1080	130	4	statistical	statistical	ADJ
eurjchem-1080	130	5	analysis	analysis	NOUN
eurjchem-1080	130	6	was	be	AUX
eurjchem-1080	130	7	studied	study	VERB
eurjchem-1080	130	8	such	such	ADJ
eurjchem-1080	130	9	as	as	ADP
eurjchem-1080	130	10	linear	linear	PROPN
eurjchem-1080	130	11	regression	regression	NOUN
eurjchem-1080	130	12	parameters	parameter	NOUN
eurjchem-1080	130	13	as	as	SCONJ
eurjchem-1080	130	14	shown	show	VERB
eurjchem-1080	130	15	in	in	ADP
eurjchem-1080	130	16	table	table	NOUN
eurjchem-1080	130	17	5	5	NUM
eurjchem-1080	130	18	and	and	CCONJ
eurjchem-1080	130	19	6	6	NUM
eurjchem-1080	130	20	.	.	PUNCT
eurjchem-1080	130	21	blind	blind	ADJ
eurjchem-1080	130	22	samples	sample	NOUN
eurjchem-1080	130	23	of	of	ADP
eurjchem-1080	130	24	pure	pure	ADJ
eurjchem-1080	130	25	sitagliptin	sitagliptin	NOUN
eurjchem-1080	130	26	phosphate	phosphate	NOUN
eurjchem-1080	130	27	of	of	ADP
eurjchem-1080	130	28	different	different	ADJ
eurjchem-1080	130	29	concentrations	concentration	NOUN
eurjchem-1080	130	30	were	be	AUX
eurjchem-1080	130	31	calculated	calculate	VERB
eurjchem-1080	130	32	from	from	ADP
eurjchem-1080	130	33	its	its	PRON
eurjchem-1080	130	34	regression	regression	NOUN
eurjchem-1080	130	35	equation	equation	NOUN
eurjchem-1080	130	36	.	.	PUNCT
eurjchem-1080	131	1	saleh	saleh	NOUN
eurjchem-1080	131	2	et	et	PROPN
eurjchem-1080	131	3	al	al	PROPN
eurjchem-1080	131	4	.	.	PUNCT
eurjchem-1080	131	5	/	/	SYM
eurjchem-1080	131	6	european	european	PROPN
eurjchem-1080	131	7	journal	journal	PROPN
eurjchem-1080	131	8	of	of	ADP
eurjchem-1080	131	9	chemistry	chemistry	NOUN
eurjchem-1080	131	10	5	5	NUM
eurjchem-1080	131	11	(	(	PUNCT
eurjchem-1080	131	12	3	3	NUM
eurjchem-1080	131	13	)	)	PUNCT
eurjchem-1080	131	14	(	(	PUNCT
eurjchem-1080	131	15	2014	2014	NUM
eurjchem-1080	131	16	)	)	PUNCT
eurjchem-1080	132	1	497‐502	497‐502	NOUN
eurjchem-1080	132	2	501	501	NUM
eurjchem-1080	132	3	table	table	NOUN
eurjchem-1080	132	4	2	2	NUM
eurjchem-1080	132	5	.	.	PUNCT
eurjchem-1080	133	1	determination	determination	NOUN
eurjchem-1080	133	2	of	of	ADP
eurjchem-1080	133	3	pure	pure	ADJ
eurjchem-1080	133	4	bulk	bulk	ADJ
eurjchem-1080	133	5	sitagliptin	sitagliptin	NOUN
eurjchem-1080	133	6	phosphate	phosphate	NOUN
eurjchem-1080	133	7	by	by	ADP
eurjchem-1080	133	8	hplc	hplc	PROPN
eurjchem-1080	133	9	.	.	PUNCT
eurjchem-1080	134	1	mixture	mixture	NOUN
eurjchem-1080	134	2	no	no	DET
eurjchem-1080	134	3	concentration	concentration	NOUN
eurjchem-1080	134	4	taken	take	VERB
eurjchem-1080	134	5	(	(	PUNCT
eurjchem-1080	134	6	µg	µg	NOUN
eurjchem-1080	134	7	/	/	SYM
eurjchem-1080	134	8	ml	ml	VERB
eurjchem-1080	134	9	)	)	PUNCT
eurjchem-1080	134	10	found	find	VERB
eurjchem-1080	134	11	(	(	PUNCT
eurjchem-1080	134	12	µg	µg	ADJ
eurjchem-1080	134	13	/	/	SYM
eurjchem-1080	134	14	ml	ml	VERB
eurjchem-1080	134	15	)	)	PUNCT
eurjchem-1080	134	16	found	find	VERB
eurjchem-1080	134	17	(	(	PUNCT
eurjchem-1080	134	18	%	%	NOUN
eurjchem-1080	134	19	)	)	PUNCT
eurjchem-1080	134	20	1	1	NUM
eurjchem-1080	134	21	150.00	150.00	NUM
eurjchem-1080	134	22	151.70	151.70	NUM
eurjchem-1080	134	23	101.13	101.13	NUM
eurjchem-1080	134	24	2	2	NUM
eurjchem-1080	134	25	300.00	300.00	NUM
eurjchem-1080	134	26	294.70	294.70	NUM
eurjchem-1080	134	27	98.23	98.23	NUM
eurjchem-1080	134	28	3	3	NUM
eurjchem-1080	134	29	500.00	500.00	NUM
eurjchem-1080	134	30	508.70	508.70	NUM
eurjchem-1080	134	31	101.74	101.74	NUM
eurjchem-1080	134	32	4	4	NUM
eurjchem-1080	134	33	800.00	800.00	NUM
eurjchem-1080	134	34	795.70	795.70	NUM
eurjchem-1080	134	35	99.46	99.46	NUM
eurjchem-1080	134	36	5	5	NUM
eurjchem-1080	134	37	1000.00	1000.00	NUM
eurjchem-1080	134	38	996.70	996.70	NUM
eurjchem-1080	135	1	99.67	99.67	NUM
eurjchem-1080	135	2	mean	mean	NOUN
eurjchem-1080	135	3	±	±	PROPN
eurjchem-1080	135	4	s.d	s.d	PROPN
eurjchem-1080	135	5	100.05±1.399	100.05±1.399	PROPN
eurjchem-1080	135	6	table	table	NOUN
eurjchem-1080	135	7	3	3	NUM
eurjchem-1080	135	8	.	.	PUNCT
eurjchem-1080	135	9	application	application	NOUN
eurjchem-1080	135	10	the	the	DET
eurjchem-1080	135	11	standard	standard	ADJ
eurjchem-1080	135	12	addition	addition	NOUN
eurjchem-1080	135	13	technique	technique	NOUN
eurjchem-1080	135	14	to	to	ADP
eurjchem-1080	135	15	the	the	DET
eurjchem-1080	135	16	analysis	analysis	NOUN
eurjchem-1080	135	17	of	of	ADP
eurjchem-1080	135	18	sitagliptin	sitagliptin	NOUN
eurjchem-1080	135	19	phosphate	phosphate	NOUN
eurjchem-1080	135	20	by	by	ADP
eurjchem-1080	135	21	hplc	hplc	NOUN
eurjchem-1080	135	22	in	in	ADP
eurjchem-1080	135	23	its	its	PRON
eurjchem-1080	135	24	tablet	tablet	ADJ
eurjchem-1080	135	25	dosage	dosage	NOUN
eurjchem-1080	135	26	form	form	NOUN
eurjchem-1080	135	27	.	.	PUNCT
eurjchem-1080	136	1	product	product	NOUN
eurjchem-1080	136	2	found	find	VERB
eurjchem-1080	136	3	(	(	PUNCT
eurjchem-1080	136	4	%	%	INTJ
eurjchem-1080	136	5	)	)	PUNCT
eurjchem-1080	136	6	pure	pure	ADJ
eurjchem-1080	136	7	added	add	VERB
eurjchem-1080	136	8	(	(	PUNCT
eurjchem-1080	136	9	µg	µg	ADJ
eurjchem-1080	136	10	/	/	SYM
eurjchem-1080	136	11	ml	ml	VERB
eurjchem-1080	136	12	)	)	PUNCT
eurjchem-1080	136	13	found	find	VERB
eurjchem-1080	136	14	(	(	PUNCT
eurjchem-1080	136	15	µg	µg	ADJ
eurjchem-1080	136	16	/	/	SYM
eurjchem-1080	136	17	ml	ml	NOUN
eurjchem-1080	136	18	)	)	PUNCT
eurjchem-1080	136	19	recovery	recovery	NOUN
eurjchem-1080	136	20	(	(	PUNCT
eurjchem-1080	136	21	%	%	INTJ
eurjchem-1080	136	22	)	)	PUNCT
eurjchem-1080	136	23	januvia	januvia	PROPN
eurjchem-1080	136	24	100	100	NUM
eurjchem-1080	136	25	mg	mg	PROPN
eurjchem-1080	136	26	sitagliptin	sitagliptin	NOUN
eurjchem-1080	136	27	phosphate	phosphate	NOUN
eurjchem-1080	136	28	/	/	SYM
eurjchem-1080	136	29	tablet	tablet	NOUN
eurjchem-1080	136	30	100.60±1.62	100.60±1.62	NUM
eurjchem-1080	136	31	100.00	100.00	NUM
eurjchem-1080	136	32	101.20	101.20	NUM
eurjchem-1080	136	33	101.20	101.20	NUM
eurjchem-1080	136	34	200.00	200.00	NUM
eurjchem-1080	136	35	199.10	199.10	NUM
eurjchem-1080	136	36	99.55	99.55	NUM
eurjchem-1080	136	37	300.00	300.00	NUM
eurjchem-1080	137	1	302.30	302.30	NUM
eurjchem-1080	137	2	100.77	100.77	NUM
eurjchem-1080	137	3	400.00	400.00	NUM
eurjchem-1080	137	4	403.60	403.60	NUM
eurjchem-1080	137	5	100.90	100.90	NUM
eurjchem-1080	137	6	500.00	500.00	NUM
eurjchem-1080	137	7	499.80	499.80	NUM
eurjchem-1080	137	8	99.96	99.96	NUM
eurjchem-1080	137	9	mean	mean	NOUN
eurjchem-1080	137	10	±	±	NUM
eurjchem-1080	137	11	s.d	s.d	PROPN
eurjchem-1080	137	12	100.48±0.69	100.48±0.69	NUM
eurjchem-1080	137	13	table	table	NOUN
eurjchem-1080	137	14	4	4	NUM
eurjchem-1080	137	15	.	.	PUNCT
eurjchem-1080	137	16	statistical	statistical	ADJ
eurjchem-1080	137	17	analysis	analysis	NOUN
eurjchem-1080	137	18	of	of	ADP
eurjchem-1080	137	19	the	the	DET
eurjchem-1080	137	20	results	result	NOUN
eurjchem-1080	137	21	obtained	obtain	VERB
eurjchem-1080	137	22	by	by	ADP
eurjchem-1080	137	23	applying	apply	VERB
eurjchem-1080	137	24	the	the	DET
eurjchem-1080	137	25	proposed	propose	VERB
eurjchem-1080	137	26	uv	uv	NOUN
eurjchem-1080	137	27	spectrophotometric	spectrophotometric	ADJ
eurjchem-1080	137	28	method	method	NOUN
eurjchem-1080	137	29	[	[	X
eurjchem-1080	137	30	16	16	NUM
eurjchem-1080	137	31	]	]	PUNCT
eurjchem-1080	137	32	for	for	ADP
eurjchem-1080	137	33	the	the	DET
eurjchem-1080	137	34	analysis	analysis	NOUN
eurjchem-1080	137	35	of	of	ADP
eurjchem-1080	137	36	pure	pure	ADJ
eurjchem-1080	137	37	sitagliptin	sitagliptin	NOUN
eurjchem-1080	137	38	phosphate	phosphate	NOUN
eurjchem-1080	137	39	.	.	PUNCT
eurjchem-1080	138	1	parameter	parameter	PROPN
eurjchem-1080	138	2	proposed	propose	VERB
eurjchem-1080	138	3	hplc	hplc	PROPN
eurjchem-1080	138	4	method	method	NOUN
eurjchem-1080	138	5	uv	uv	NOUN
eurjchem-1080	138	6	spectrophotometric	spectrophotometric	ADJ
eurjchem-1080	138	7	method	method	NOUN
eurjchem-1080	138	8	mean	mean	ADJ
eurjchem-1080	138	9	±s.d	±s.d	PROPN
eurjchem-1080	138	10	100.05±1.399	100.05±1.399	NOUN
eurjchem-1080	139	1	99.88±0.899	99.88±0.899	X
eurjchem-1080	139	2	na	na	PART
eurjchem-1080	139	3	5	5	NUM
eurjchem-1080	139	4	5	5	NUM
eurjchem-1080	139	5	t	t	NOUN
eurjchem-1080	139	6	0.251	0.251	NUM
eurjchem-1080	139	7	(	(	PUNCT
eurjchem-1080	139	8	2.306	2.306	NUM
eurjchem-1080	139	9	)	)	PUNCT
eurjchem-1080	139	10	b	b	NOUN
eurjchem-1080	139	11	‐	‐	ADP
eurjchem-1080	139	12	f	f	NOUN
eurjchem-1080	139	13	2.422	2.422	NUM
eurjchem-1080	139	14	(	(	PUNCT
eurjchem-1080	139	15	6.390	6.390	NUM
eurjchem-1080	139	16	)	)	PUNCT
eurjchem-1080	139	17	b	b	NOUN
eurjchem-1080	139	18	‐	‐	NOUN
eurjchem-1080	139	19	a	a	DET
eurjchem-1080	139	20	n	n	NOUN
eurjchem-1080	139	21	:	:	PUNCT
eurjchem-1080	139	22	number	number	NOUN
eurjchem-1080	139	23	of	of	ADP
eurjchem-1080	139	24	determinations	determination	NOUN
eurjchem-1080	139	25	.	.	PUNCT
eurjchem-1080	140	1	b	b	X
eurjchem-1080	140	2	the	the	DET
eurjchem-1080	140	3	values	value	NOUN
eurjchem-1080	140	4	in	in	ADP
eurjchem-1080	140	5	parentheses	parenthesis	NOUN
eurjchem-1080	140	6	are	be	AUX
eurjchem-1080	140	7	corresponding	correspond	VERB
eurjchem-1080	140	8	to	to	ADP
eurjchem-1080	140	9	the	the	DET
eurjchem-1080	140	10	theoretical	theoretical	ADJ
eurjchem-1080	140	11	values	value	NOUN
eurjchem-1080	140	12	of	of	ADP
eurjchem-1080	140	13	t	t	PROPN
eurjchem-1080	140	14	and	and	CCONJ
eurjchem-1080	140	15	f	f	PROPN
eurjchem-1080	140	16	at	at	ADP
eurjchem-1080	140	17	(	(	PUNCT
eurjchem-1080	140	18	p	p	X
eurjchem-1080	140	19	=	=	NOUN
eurjchem-1080	140	20	0.05	0.05	NUM
eurjchem-1080	140	21	)	)	PUNCT
eurjchem-1080	140	22	.	.	PUNCT
eurjchem-1080	141	1	table	table	NOUN
eurjchem-1080	141	2	5	5	NUM
eurjchem-1080	141	3	.	.	PUNCT
eurjchem-1080	142	1	linear	linear	PROPN
eurjchem-1080	142	2	regression	regression	NOUN
eurjchem-1080	142	3	data	datum	NOUN
eurjchem-1080	142	4	,	,	PUNCT
eurjchem-1080	142	5	anova	anova	X
eurjchem-1080	142	6	a	a	PRON
eurjchem-1080	142	7	of	of	ADP
eurjchem-1080	142	8	regression	regression	NOUN
eurjchem-1080	142	9	.	.	PUNCT
eurjchem-1080	143	1	model	model	PROPN
eurjchem-1080	143	2	sum	sum	NOUN
eurjchem-1080	143	3	of	of	ADP
eurjchem-1080	143	4	squares	square	NOUN
eurjchem-1080	143	5	df	df	PROPN
eurjchem-1080	143	6	mean	mean	PROPN
eurjchem-1080	143	7	square	square	PROPN
eurjchem-1080	143	8	f	f	PROPN
eurjchem-1080	143	9	sigma	sigma	VERB
eurjchem-1080	143	10	mixture	mixture	NOUN
eurjchem-1080	143	11	no	no	NOUN
eurjchem-1080	143	12	:	:	SYM
eurjchem-1080	143	13	1	1	NUM
eurjchem-1080	143	14	regression	regression	VERB
eurjchem-1080	143	15	0.720	0.720	NUM
eurjchem-1080	143	16	1	1	NUM
eurjchem-1080	143	17	0.720	0.720	NUM
eurjchem-1080	143	18	11335.665	11335.665	NUM
eurjchem-1080	143	19	0.000	0.000	NUM
eurjchem-1080	143	20	b	b	NOUN
eurjchem-1080	143	21	residual	residual	ADJ
eurjchem-1080	143	22	0.000	0.000	NUM
eurjchem-1080	143	23	5	5	NUM
eurjchem-1080	143	24	0.000	0.000	NUM
eurjchem-1080	143	25	total	total	NOUN
eurjchem-1080	143	26	0.720	0.720	NUM
eurjchem-1080	143	27	6	6	NUM
eurjchem-1080	143	28	a	a	DET
eurjchem-1080	143	29	dependent	dependent	ADJ
eurjchem-1080	143	30	variable	variable	NOUN
eurjchem-1080	143	31	:	:	PUNCT
eurjchem-1080	143	32	area	area	NOUN
eurjchem-1080	143	33	.	.	PUNCT
eurjchem-1080	144	1	b	b	NOUN
eurjchem-1080	144	2	predictors	predictor	NOUN
eurjchem-1080	144	3	:	:	PUNCT
eurjchem-1080	144	4	(	(	PUNCT
eurjchem-1080	144	5	constant	constant	ADJ
eurjchem-1080	144	6	)	)	PUNCT
eurjchem-1080	144	7	,	,	PUNCT
eurjchem-1080	144	8	conc	conc	NOUN
eurjchem-1080	144	9	.	.	PUNCT
eurjchem-1080	144	10	µg	µg	VERB
eurjchem-1080	144	11	/	/	SYM
eurjchem-1080	144	12	ml	ml	NOUN
eurjchem-1080	144	13	.	.	NOUN
eurjchem-1080	144	14	table	table	NOUN
eurjchem-1080	144	15	6	6	NUM
eurjchem-1080	144	16	.	.	PUNCT
eurjchem-1080	145	1	linear	linear	PROPN
eurjchem-1080	145	2	regression	regression	PROPN
eurjchem-1080	145	3	data	datum	NOUN
eurjchem-1080	145	4	,	,	PUNCT
eurjchem-1080	145	5	coefficients	coefficient	NOUN
eurjchem-1080	145	6	a.	a.	NOUN
eurjchem-1080	145	7	model	model	NOUN
eurjchem-1080	145	8	unstandardized	unstandardized	ADJ
eurjchem-1080	145	9	coefficients	coefficient	NOUN
eurjchem-1080	145	10	standardized	standardized	ADJ
eurjchem-1080	145	11	coefficients	coefficient	NOUN
eurjchem-1080	145	12	t	t	PROPN
eurjchem-1080	145	13	sigma	sigma	NOUN
eurjchem-1080	145	14	95	95	NUM
eurjchem-1080	145	15	%	%	NOUN
eurjchem-1080	145	16	confidence	confidence	NOUN
eurjchem-1080	145	17	interval	interval	NOUN
eurjchem-1080	145	18	for	for	ADP
eurjchem-1080	145	19	b	b	PROPN
eurjchem-1080	145	20	b	b	PROPN
eurjchem-1080	145	21	standard	standard	ADJ
eurjchem-1080	145	22	error	error	NOUN
eurjchem-1080	145	23	beta	beta	NOUN
eurjchem-1080	145	24	lower	lower	ADV
eurjchem-1080	145	25	bound	bind	VERB
eurjchem-1080	145	26	upper	upper	ADJ
eurjchem-1080	145	27	bound	bind	VERB
eurjchem-1080	145	28	mixture	mixture	NOUN
eurjchem-1080	145	29	no	no	NOUN
eurjchem-1080	145	30	:	:	SYM
eurjchem-1080	145	31	1	1	NUM
eurjchem-1080	145	32	constant	constant	ADJ
eurjchem-1080	145	33	0.003	0.003	NUM
eurjchem-1080	145	34	0.005	0.005	NUM
eurjchem-1080	145	35	0.658	0.658	NUM
eurjchem-1080	145	36	0.539	0.539	NUM
eurjchem-1080	145	37	‐0.010	‐0.010	NOUN
eurjchem-1080	145	38	0.016	0.016	NUM
eurjchem-1080	145	39	conc	conc	NOUN
eurjchem-1080	145	40	.	.	PUNCT
eurjchem-1080	146	1	µg	µg	VERB
eurjchem-1080	146	2	/	/	SYM
eurjchem-1080	146	3	ml	ml	ADP
eurjchem-1080	146	4	0.001	0.001	NUM
eurjchem-1080	146	5	0.000	0.000	NUM
eurjchem-1080	146	6	1.000	1.000	NUM
eurjchem-1080	146	7	106.469	106.469	NUM
eurjchem-1080	146	8	0.000	0.000	NUM
eurjchem-1080	146	9	0.001	0.001	NUM
eurjchem-1080	146	10	0.001	0.001	NUM
eurjchem-1080	146	11	a	a	DET
eurjchem-1080	146	12	dependent	dependent	ADJ
eurjchem-1080	146	13	variable	variable	NOUN
eurjchem-1080	146	14	:	:	PUNCT
eurjchem-1080	146	15	area	area	NOUN
eurjchem-1080	146	16	.	.	PUNCT
eurjchem-1080	147	1	the	the	DET
eurjchem-1080	147	2	degree	degree	NOUN
eurjchem-1080	147	3	of	of	ADP
eurjchem-1080	147	4	method	method	ADJ
eurjchem-1080	147	5	repeatability	repeatability	NOUN
eurjchem-1080	147	6	(	(	PUNCT
eurjchem-1080	147	7	intra‐day	intra‐day	NOUN
eurjchem-1080	147	8	)	)	PUNCT
eurjchem-1080	147	9	and	and	CCONJ
eurjchem-1080	147	10	inter‐	inter‐	NOUN
eurjchem-1080	147	11	mediate	mediate	PROPN
eurjchem-1080	147	12	precision	precision	NOUN
eurjchem-1080	147	13	(	(	PUNCT
eurjchem-1080	147	14	inter‐days	inter‐day	NOUN
eurjchem-1080	147	15	)	)	PUNCT
eurjchem-1080	147	16	were	be	AUX
eurjchem-1080	147	17	measured	measure	VERB
eurjchem-1080	147	18	by	by	ADP
eurjchem-1080	147	19	analysing	analyse	VERB
eurjchem-1080	147	20	each	each	DET
eurjchem-1080	147	21	concentration	concentration	NOUN
eurjchem-1080	147	22	of	of	ADP
eurjchem-1080	147	23	sitagliptin	sitagliptin	NOUN
eurjchem-1080	147	24	phosphate	phosphate	NOUN
eurjchem-1080	147	25	four	four	NUM
eurjchem-1080	147	26	times	time	NOUN
eurjchem-1080	147	27	by	by	ADP
eurjchem-1080	147	28	the	the	DET
eurjchem-1080	147	29	proposed	propose	VERB
eurjchem-1080	147	30	method	method	NOUN
eurjchem-1080	147	31	in	in	ADP
eurjchem-1080	147	32	the	the	DET
eurjchem-1080	147	33	same	same	ADJ
eurjchem-1080	147	34	day	day	NOUN
eurjchem-1080	147	35	and	and	CCONJ
eurjchem-1080	147	36	for	for	ADP
eurjchem-1080	147	37	four	four	NUM
eurjchem-1080	147	38	days	day	NOUN
eurjchem-1080	147	39	,	,	PUNCT
eurjchem-1080	147	40	then	then	ADV
eurjchem-1080	147	41	calculating	calculate	VERB
eurjchem-1080	147	42	%	%	NOUN
eurjchem-1080	147	43	r.s.d	r.s.d	NOUN
eurjchem-1080	147	44	.	.	PUNCT
eurjchem-1080	148	1	values	value	NOUN
eurjchem-1080	148	2	which	which	PRON
eurjchem-1080	148	3	were	be	AUX
eurjchem-1080	148	4	0.53	0.53	NUM
eurjchem-1080	148	5	and	and	CCONJ
eurjchem-1080	148	6	0.74	0.74	NUM
eurjchem-1080	148	7	,	,	PUNCT
eurjchem-1080	148	8	respectively	respectively	ADV
eurjchem-1080	148	9	.	.	PUNCT
eurjchem-1080	149	1	the	the	DET
eurjchem-1080	149	2	results	result	NOUN
eurjchem-1080	149	3	of	of	ADP
eurjchem-1080	149	4	the	the	DET
eurjchem-1080	149	5	proposed	propose	VERB
eurjchem-1080	149	6	method	method	NOUN
eurjchem-1080	149	7	showed	show	VERB
eurjchem-1080	149	8	that	that	SCONJ
eurjchem-1080	149	9	it	it	PRON
eurjchem-1080	149	10	is	be	AUX
eurjchem-1080	149	11	accurate	accurate	ADJ
eurjchem-1080	149	12	,	,	PUNCT
eurjchem-1080	149	13	precise	precise	ADJ
eurjchem-1080	149	14	,	,	PUNCT
eurjchem-1080	149	15	specific	specific	ADJ
eurjchem-1080	149	16	,	,	PUNCT
eurjchem-1080	149	17	and	and	CCONJ
eurjchem-1080	149	18	rugged	rugged	ADJ
eurjchem-1080	149	19	according	accord	VERB
eurjchem-1080	149	20	to	to	ADP
eurjchem-1080	149	21	the	the	DET
eurjchem-1080	149	22	%	%	NOUN
eurjchem-1080	149	23	r.s.d	r.s.d	NOUN
eurjchem-1080	149	24	.	.	PUNCT
eurjchem-1080	150	1	values	value	NOUN
eurjchem-1080	150	2	of	of	ADP
eurjchem-1080	150	3	intra‐day	intra‐day	NOUN
eurjchem-1080	150	4	and	and	CCONJ
eurjchem-1080	150	5	inter‐day	inter‐day	PROPN
eurjchem-1080	150	6	determinations	determination	NOUN
eurjchem-1080	150	7	.	.	PUNCT
eurjchem-1080	151	1	4	4	X
eurjchem-1080	151	2	.	.	X
eurjchem-1080	151	3	conclusion	conclusion	NOUN
eurjchem-1080	151	4	a	a	DET
eurjchem-1080	151	5	validated	validate	VERB
eurjchem-1080	151	6	stability‐indicating	stability‐indicate	VERB
eurjchem-1080	151	7	hplc	hplc	NOUN
eurjchem-1080	151	8	analytical	analytical	ADJ
eurjchem-1080	151	9	method	method	NOUN
eurjchem-1080	151	10	has	have	AUX
eurjchem-1080	151	11	been	be	AUX
eurjchem-1080	151	12	developed	develop	VERB
eurjchem-1080	151	13	for	for	ADP
eurjchem-1080	151	14	the	the	DET
eurjchem-1080	151	15	determination	determination	NOUN
eurjchem-1080	151	16	of	of	ADP
eurjchem-1080	151	17	sitagliptin	sitagliptin	NOUN
eurjchem-1080	151	18	phosphate	phosphate	NOUN
eurjchem-1080	151	19	in	in	ADP
eurjchem-1080	151	20	pure	pure	ADJ
eurjchem-1080	151	21	form	form	NOUN
eurjchem-1080	151	22	and	and	CCONJ
eurjchem-1080	151	23	in	in	ADP
eurjchem-1080	151	24	tablet	tablet	ADJ
eurjchem-1080	151	25	dosage	dosage	NOUN
eurjchem-1080	151	26	formulation	formulation	NOUN
eurjchem-1080	151	27	.	.	PUNCT
eurjchem-1080	152	1	all	all	DET
eurjchem-1080	152	2	the	the	DET
eurjchem-1080	152	3	validation	validation	NOUN
eurjchem-1080	152	4	parameters	parameter	NOUN
eurjchem-1080	152	5	were	be	AUX
eurjchem-1080	152	6	studied	study	VERB
eurjchem-1080	152	7	on	on	ADP
eurjchem-1080	152	8	poroshell	poroshell	PROPN
eurjchem-1080	152	9	120	120	NUM
eurjchem-1080	152	10	ec‐c18	ec‐c18	NOUN
eurjchem-1080	152	11	column	column	NOUN
eurjchem-1080	152	12	which	which	PRON
eurjchem-1080	152	13	achieved	achieve	VERB
eurjchem-1080	152	14	the	the	DET
eurjchem-1080	152	15	best	good	ADJ
eurjchem-1080	152	16	separation	separation	NOUN
eurjchem-1080	152	17	.	.	PUNCT
eurjchem-1080	153	1	the	the	DET
eurjchem-1080	153	2	results	result	NOUN
eurjchem-1080	153	3	of	of	ADP
eurjchem-1080	153	4	stress	stress	NOUN
eurjchem-1080	153	5	testing	testing	NOUN
eurjchem-1080	153	6	were	be	AUX
eurjchem-1080	153	7	under	under	ADP
eurjchem-1080	153	8	taken	take	VERB
eurjchem-1080	153	9	according	accord	VERB
eurjchem-1080	153	10	to	to	ADP
eurjchem-1080	153	11	the	the	DET
eurjchem-1080	153	12	international	international	ADJ
eurjchem-1080	153	13	conference	conference	NOUN
eurjchem-1080	153	14	on	on	ADP
eurjchem-1080	153	15	harmonization	harmonization	NOUN
eurjchem-1080	153	16	(	(	PUNCT
eurjchem-1080	153	17	ich	ich	NOUN
eurjchem-1080	153	18	)	)	PUNCT
eurjchem-1080	153	19	guidelines	guideline	NOUN
eurjchem-1080	153	20	,	,	PUNCT
eurjchem-1080	153	21	which	which	PRON
eurjchem-1080	153	22	revealed	reveal	VERB
eurjchem-1080	153	23	that	that	SCONJ
eurjchem-1080	153	24	the	the	DET
eurjchem-1080	153	25	studied	study	VERB
eurjchem-1080	153	26	method	method	NOUN
eurjchem-1080	153	27	is	be	AUX
eurjchem-1080	153	28	selective	selective	ADJ
eurjchem-1080	153	29	and	and	CCONJ
eurjchem-1080	153	30	stability‐indicating	stability‐indicate	VERB
eurjchem-1080	153	31	.	.	PUNCT
eurjchem-1080	154	1	the	the	DET
eurjchem-1080	154	2	propo‐	propo‐	ADJ
eurjchem-1080	154	3	sed	sed	ADJ
eurjchem-1080	154	4	method	method	NOUN
eurjchem-1080	154	5	has	have	AUX
eurjchem-1080	154	6	been	be	AUX
eurjchem-1080	154	7	found	find	VERB
eurjchem-1080	154	8	to	to	PART
eurjchem-1080	154	9	have	have	VERB
eurjchem-1080	154	10	the	the	DET
eurjchem-1080	154	11	required	require	VERB
eurjchem-1080	154	12	accuracy	accuracy	NOUN
eurjchem-1080	154	13	,	,	PUNCT
eurjchem-1080	154	14	selectivity	selectivity	NOUN
eurjchem-1080	154	15	,	,	PUNCT
eurjchem-1080	154	16	sensitivity	sensitivity	NOUN
eurjchem-1080	154	17	,	,	PUNCT
eurjchem-1080	154	18	and	and	CCONJ
eurjchem-1080	154	19	precision	precision	NOUN
eurjchem-1080	154	20	to	to	PART
eurjchem-1080	154	21	assay	assay	VERB
eurjchem-1080	154	22	sitagliptin	sitagliptin	NOUN
eurjchem-1080	154	23	phosphate	phosphate	NOUN
eurjchem-1080	154	24	in	in	ADP
eurjchem-1080	154	25	bulk	bulk	ADJ
eurjchem-1080	154	26	form	form	NOUN
eurjchem-1080	154	27	and	and	CCONJ
eurjchem-1080	154	28	in	in	ADP
eurjchem-1080	154	29	a	a	DET
eurjchem-1080	154	30	pharmaceutical	pharmaceutical	ADJ
eurjchem-1080	154	31	dosage	dosage	NOUN
eurjchem-1080	154	32	form	form	NOUN
eurjchem-1080	154	33	.	.	PUNCT
eurjchem-1080	155	1	degradation	degradation	NOUN
eurjchem-1080	155	2	products	product	NOUN
eurjchem-1080	155	3	resulting	result	VERB
eurjchem-1080	155	4	from	from	ADP
eurjchem-1080	155	5	the	the	DET
eurjchem-1080	155	6	stress	stress	NOUN
eurjchem-1080	155	7	studies	study	NOUN
eurjchem-1080	155	8	and	and	CCONJ
eurjchem-1080	155	9	the	the	DET
eurjchem-1080	155	10	excipients	excipient	NOUN
eurjchem-1080	155	11	found	find	VERB
eurjchem-1080	155	12	in	in	ADP
eurjchem-1080	155	13	the	the	DET
eurjchem-1080	155	14	tablet	tablet	NOUN
eurjchem-1080	155	15	dosage	dosage	NOUN
eurjchem-1080	155	16	forms	form	NOUN
eurjchem-1080	155	17	did	do	AUX
eurjchem-1080	155	18	not	not	PART
eurjchem-1080	155	19	interfere	interfere	VERB
eurjchem-1080	155	20	with	with	ADP
eurjchem-1080	155	21	the	the	DET
eurjchem-1080	155	22	detection	detection	NOUN
eurjchem-1080	155	23	of	of	ADP
eurjchem-1080	155	24	sitagliptin	sitagliptin	NOUN
eurjchem-1080	155	25	phosphate	phosphate	NOUN
eurjchem-1080	155	26	which	which	PRON
eurjchem-1080	155	27	indicates	indicate	VERB
eurjchem-1080	155	28	that	that	SCONJ
eurjchem-1080	155	29	the	the	DET
eurjchem-1080	155	30	assay	assay	NOUN
eurjchem-1080	155	31	are	be	AUX
eurjchem-1080	155	32	stability‐indicating	stability‐indicate	VERB
eurjchem-1080	155	33	assay	assay	NOUN
eurjchem-1080	155	34	.	.	PUNCT
eurjchem-1080	156	1	the	the	DET
eurjchem-1080	156	2	achieved	achieve	VERB
eurjchem-1080	156	3	methods	method	NOUN
eurjchem-1080	156	4	are	be	AUX
eurjchem-1080	156	5	suitable	suitable	ADJ
eurjchem-1080	156	6	for	for	ADP
eurjchem-1080	156	7	the	the	DET
eurjchem-1080	156	8	routine	routine	ADJ
eurjchem-1080	156	9	analysis	analysis	NOUN
eurjchem-1080	156	10	of	of	ADP
eurjchem-1080	156	11	sitagliptin	sitagliptin	NOUN
eurjchem-1080	156	12	phosphate	phosphate	NOUN
eurjchem-1080	156	13	in	in	ADP
eurjchem-1080	156	14	either	either	CCONJ
eurjchem-1080	156	15	bulk	bulk	ADJ
eurjchem-1080	156	16	powder	powder	NOUN
eurjchem-1080	156	17	or	or	CCONJ
eurjchem-1080	156	18	in	in	ADP
eurjchem-1080	156	19	pharma‐ceutical	pharma‐ceutical	ADJ
eurjchem-1080	156	20	dosage	dosage	NOUN
eurjchem-1080	156	21	forms	form	NOUN
eurjchem-1080	156	22	.	.	PUNCT
eurjchem-1080	157	1	the	the	DET
eurjchem-1080	157	2	simplicity	simplicity	NOUN
eurjchem-1080	157	3	of	of	ADP
eurjchem-1080	157	4	the	the	DET
eurjchem-1080	157	5	applied	apply	VERB
eurjchem-1080	157	6	method	method	NOUN
eurjchem-1080	157	7	allows	allow	VERB
eurjchem-1080	157	8	their	their	PRON
eurjchem-1080	157	9	application	application	NOUN
eurjchem-1080	157	10	in	in	ADP
eurjchem-1080	157	11	quality	quality	NOUN
eurjchem-1080	157	12	control	control	NOUN
eurjchem-1080	157	13	laboratories	laboratory	NOUN
eurjchem-1080	157	14	.	.	PUNCT
eurjchem-1080	158	1	acknowledgements	acknowledgement	NOUN
eurjchem-1080	158	2	the	the	DET
eurjchem-1080	158	3	authors	author	NOUN
eurjchem-1080	158	4	are	be	AUX
eurjchem-1080	158	5	sincerely	sincerely	ADV
eurjchem-1080	158	6	indebted	indebted	ADJ
eurjchem-1080	158	7	and	and	CCONJ
eurjchem-1080	158	8	grateful	grateful	ADJ
eurjchem-1080	158	9	to	to	ADP
eurjchem-1080	158	10	dr	dr	PROPN
eurjchem-1080	158	11	.	.	PROPN
eurjchem-1080	158	12	mohamed	mohamed	PROPN
eurjchem-1080	158	13	nabil	nabil	PROPN
eurjchem-1080	158	14	aboul‐enein	aboul‐enein	PROPN
eurjchem-1080	158	15	,	,	PUNCT
eurjchem-1080	158	16	professor	professor	NOUN
eurjchem-1080	158	17	of	of	ADP
eurjchem-1080	158	18	pharmaceutical	pharmaceutical	ADJ
eurjchem-1080	158	19	chemistry	chemistry	NOUN
eurjchem-1080	158	20	,	,	PUNCT
eurjchem-1080	158	21	department	department	NOUN
eurjchem-1080	158	22	of	of	ADP
eurjchem-1080	158	23	pharmaceutical	pharmaceutical	NOUN
eurjchem-1080	158	24	and	and	CCONJ
eurjchem-1080	158	25	medicinal	medicinal	ADJ
eurjchem-1080	158	26	chemistry	chemistry	NOUN
eurjchem-1080	158	27	,	,	PUNCT
eurjchem-1080	158	28	national	national	ADJ
eurjchem-1080	158	29	research	research	NOUN
eurjchem-1080	158	30	centre	centre	NOUN
eurjchem-1080	158	31	,	,	PUNCT
eurjchem-1080	158	32	for	for	ADP
eurjchem-1080	158	33	his	his	PRON
eurjchem-1080	158	34	endless	endless	ADJ
eurjchem-1080	158	35	support	support	NOUN
eurjchem-1080	158	36	,	,	PUNCT
eurjchem-1080	158	37	guidance	guidance	NOUN
eurjchem-1080	158	38	and	and	CCONJ
eurjchem-1080	158	39	unlimited	unlimited	ADJ
eurjchem-1080	158	40	valuable	valuable	ADJ
eurjchem-1080	158	41	advice	advice	NOUN
eurjchem-1080	158	42	throughout	throughout	ADP
eurjchem-1080	158	43	this	this	DET
eurjchem-1080	158	44	work	work	NOUN
eurjchem-1080	158	45	.	.	PUNCT
eurjchem-1080	159	1	references	reference	NOUN
eurjchem-1080	159	2	[	[	X
eurjchem-1080	159	3	1	1	NUM
eurjchem-1080	159	4	]	]	PUNCT
eurjchem-1080	159	5	.	.	PUNCT
eurjchem-1080	160	1	herman	herman	PROPN
eurjchem-1080	160	2	,	,	PUNCT
eurjchem-1080	160	3	g.	g.	PROPN
eurjchem-1080	160	4	a.	a.	PROPN
eurjchem-1080	160	5	;	;	PUNCT
eurjchem-1080	160	6	stevens	stevens	PROPN
eurjchem-1080	160	7	,	,	PUNCT
eurjchem-1080	160	8	c.	c.	PROPN
eurjchem-1080	160	9	;	;	PUNCT
eurjchem-1080	160	10	dyck	dyck	PROPN
eurjchem-1080	160	11	,	,	PUNCT
eurjchem-1080	160	12	k.	k.	PROPN
eurjchem-1080	160	13	v.	v.	PROPN
eurjchem-1080	160	14	;	;	PUNCT
eurjchem-1080	160	15	bergman	bergman	PROPN
eurjchem-1080	160	16	,	,	PUNCT
eurjchem-1080	160	17	a.	a.	NOUN
eurjchem-1080	160	18	;	;	PUNCT
eurjchem-1080	160	19	yi	yi	PROPN
eurjchem-1080	160	20	,	,	PUNCT
eurjchem-1080	160	21	b.	b.	PROPN
eurjchem-1080	160	22	;	;	PUNCT
eurjchem-1080	160	23	de	de	PROPN
eurjchem-1080	160	24	smet	smet	PROPN
eurjchem-1080	160	25	,	,	PUNCT
eurjchem-1080	160	26	m.	m.	NOUN
eurjchem-1080	160	27	;	;	PUNCT
eurjchem-1080	160	28	snyder	snyder	PROPN
eurjchem-1080	160	29	,	,	PUNCT
eurjchem-1080	160	30	k.	k.	PROPN
eurjchem-1080	160	31	;	;	PUNCT
eurjchem-1080	160	32	hilliard	hilliard	PROPN
eurjchem-1080	160	33	,	,	PUNCT
eurjchem-1080	160	34	d.	d.	PROPN
eurjchem-1080	160	35	;	;	PUNCT
eurjchem-1080	160	36	tanen	tanen	NOUN
eurjchem-1080	160	37	,	,	PUNCT
eurjchem-1080	160	38	m.	m.	NOUN
eurjchem-1080	160	39	;	;	PUNCT
eurjchem-1080	160	40	tanaka	tanaka	PROPN
eurjchem-1080	160	41	,	,	PUNCT
eurjchem-1080	160	42	w.	w.	PROPN
eurjchem-1080	160	43	;	;	PUNCT
eurjchem-1080	160	44	wang	wang	PROPN
eurjchem-1080	160	45	,	,	PUNCT
eurjchem-1080	160	46	a.	a.	PROPN
eurjchem-1080	160	47	q.	q.	PROPN
eurjchem-1080	160	48	;	;	PUNCT
eurjchem-1080	160	49	zeng	zeng	PROPN
eurjchem-1080	160	50	,	,	PUNCT
eurjchem-1080	160	51	w.	w.	PROPN
eurjchem-1080	160	52	;	;	PUNCT
eurjchem-1080	160	53	musson	musson	PROPN
eurjchem-1080	160	54	,	,	PUNCT
eurjchem-1080	160	55	d.	d.	PROPN
eurjchem-1080	160	56	;	;	PUNCT
eurjchem-1080	160	57	winchell	winchell	PROPN
eurjchem-1080	160	58	,	,	PUNCT
eurjchem-1080	160	59	g.	g.	PROPN
eurjchem-1080	160	60	;	;	PUNCT
eurjchem-1080	160	61	davis	davis	PROPN
eurjchem-1080	160	62	,	,	PUNCT
eurjchem-1080	160	63	m.	m.	PROPN
eurjchem-1080	160	64	j.	j.	PROPN
eurjchem-1080	160	65	;	;	PUNCT
eurjchem-1080	160	66	ramael	ramael	PROPN
eurjchem-1080	160	67	,	,	PUNCT
eurjchem-1080	160	68	s.	s.	PROPN
eurjchem-1080	160	69	;	;	PUNCT
eurjchem-1080	160	70	gottesdiener	gottesdiener	PROPN
eurjchem-1080	160	71	,	,	PUNCT
eurjchem-1080	160	72	k.	k.	PROPN
eurjchem-1080	160	73	m.	m.	PROPN
eurjchem-1080	160	74	;	;	PUNCT
eurjchem-1080	160	75	wagner	wagner	PROPN
eurjchem-1080	160	76	,	,	PUNCT
eurjchem-1080	160	77	j.	j.	PROPN
eurjchem-1080	160	78	clin	clin	PROPN
eurjchem-1080	160	79	.	.	PUNCT
eurjchem-1080	161	1	pharmacol	pharmacol	PROPN
eurjchem-1080	161	2	.	.	PUNCT
eurjchem-1080	162	1	ther	ther	PROPN
eurjchem-1080	162	2	.	.	PUNCT
eurjchem-1080	163	1	2005	2005	NUM
eurjchem-1080	163	2	,	,	PUNCT
eurjchem-1080	163	3	78	78	NUM
eurjchem-1080	163	4	,	,	PUNCT
eurjchem-1080	163	5	675‐688	675‐688	NOUN
eurjchem-1080	163	6	.	.	PUNCT
eurjchem-1080	164	1	[	[	X
eurjchem-1080	164	2	2	2	NUM
eurjchem-1080	164	3	]	]	PUNCT
eurjchem-1080	164	4	.	.	PUNCT
eurjchem-1080	165	1	amori	amori	PROPN
eurjchem-1080	165	2	,	,	PUNCT
eurjchem-1080	165	3	r.	r.	PROPN
eurjchem-1080	165	4	e.	e.	PROPN
eurjchem-1080	165	5	;	;	PUNCT
eurjchem-1080	165	6	lau	lau	PROPN
eurjchem-1080	165	7	,	,	PUNCT
eurjchem-1080	165	8	j.	j.	PROPN
eurjchem-1080	165	9	;	;	PUNCT
eurjchem-1080	165	10	pittas	pitta	NOUN
eurjchem-1080	165	11	,	,	PUNCT
eurjchem-1080	165	12	a.	a.	NOUN
eurjchem-1080	165	13	g.	g.	PROPN
eurjchem-1080	165	14	jama	jama	PROPN
eurjchem-1080	165	15	2007	2007	NUM
eurjchem-1080	165	16	,	,	PUNCT
eurjchem-1080	165	17	298	298	NUM
eurjchem-1080	165	18	,	,	PUNCT
eurjchem-1080	165	19	194‐206	194‐206	NUM
eurjchem-1080	165	20	.	.	PUNCT
eurjchem-1080	166	1	[	[	X
eurjchem-1080	166	2	3	3	NUM
eurjchem-1080	166	3	]	]	PUNCT
eurjchem-1080	166	4	.	.	PUNCT
eurjchem-1080	167	1	rosenstok	rosenstok	PROPN
eurjchem-1080	167	2	,	,	PUNCT
eurjchem-1080	167	3	j.	j.	PROPN
eurjchem-1080	167	4	;	;	PUNCT
eurjchem-1080	167	5	sankoh	sankoh	PROPN
eurjchem-1080	167	6	,	,	PUNCT
eurjchem-1080	167	7	s.	s.	PROPN
eurjchem-1080	167	8	;	;	PUNCT
eurjchem-1080	167	9	list	list	NOUN
eurjchem-1080	167	10	,	,	PUNCT
eurjchem-1080	167	11	j.	j.	PROPN
eurjchem-1080	167	12	f.	f.	PROPN
eurjchem-1080	167	13	diabetes	diabetes	PROPN
eurjchem-1080	167	14	obes	obe	NOUN
eurjchem-1080	167	15	.	.	PUNCT
eurjchem-1080	168	1	metab	metab	NOUN
eurjchem-1080	168	2	.	.	PUNCT
eurjchem-1080	169	1	2008	2008	NUM
eurjchem-1080	169	2	,	,	PUNCT
eurjchem-1080	169	3	10	10	NUM
eurjchem-1080	169	4	,	,	PUNCT
eurjchem-1080	169	5	376‐	376‐	PROPN
eurjchem-1080	169	6	386	386	NUM
eurjchem-1080	169	7	.	.	PUNCT
eurjchem-1080	170	1	[	[	X
eurjchem-1080	170	2	4	4	NUM
eurjchem-1080	170	3	]	]	PUNCT
eurjchem-1080	170	4	.	.	PUNCT
eurjchem-1080	171	1	herman	herman	PROPN
eurjchem-1080	171	2	,	,	PUNCT
eurjchem-1080	171	3	g.	g.	PROPN
eurjchem-1080	171	4	a.	a.	PROPN
eurjchem-1080	171	5	;	;	PUNCT
eurjchem-1080	171	6	bergman	bergman	PROPN
eurjchem-1080	171	7	,	,	PUNCT
eurjchem-1080	171	8	a.	a.	PROPN
eurjchem-1080	171	9	;	;	PUNCT
eurjchem-1080	171	10	liu	liu	PROPN
eurjchem-1080	171	11	,	,	PUNCT
eurjchem-1080	171	12	f.	f.	PROPN
eurjchem-1080	171	13	;	;	PUNCT
eurjchem-1080	171	14	stevens	stevens	PROPN
eurjchem-1080	171	15	,	,	PUNCT
eurjchem-1080	171	16	c.	c.	PROPN
eurjchem-1080	171	17	;	;	PUNCT
eurjchem-1080	171	18	wang	wang	PROPN
eurjchem-1080	171	19	,	,	PUNCT
eurjchem-1080	171	20	a.	a.	PROPN
eurjchem-1080	171	21	q.	q.	PROPN
eurjchem-1080	171	22	;	;	PUNCT
eurjchem-1080	171	23	zeng	zeng	PROPN
eurjchem-1080	171	24	,	,	PUNCT
eurjchem-1080	171	25	w.	w.	PROPN
eurjchem-1080	171	26	;	;	PUNCT
eurjchem-1080	171	27	chen	chen	PROPN
eurjchem-1080	171	28	,	,	PUNCT
eurjchem-1080	171	29	l.	l.	PROPN
eurjchem-1080	171	30	;	;	PUNCT
eurjchem-1080	171	31	snyder	snyder	PROPN
eurjchem-1080	171	32	,	,	PUNCT
eurjchem-1080	171	33	k.	k.	PROPN
eurjchem-1080	171	34	;	;	PUNCT
eurjchem-1080	171	35	hilliard	hilliard	PROPN
eurjchem-1080	171	36	,	,	PUNCT
eurjchem-1080	171	37	d.	d.	PROPN
eurjchem-1080	171	38	;	;	PUNCT
eurjchem-1080	171	39	tanen	tanen	NOUN
eurjchem-1080	171	40	,	,	PUNCT
eurjchem-1080	171	41	m.	m.	NOUN
eurjchem-1080	171	42	;	;	PUNCT
eurjchem-1080	171	43	tanaka	tanaka	PROPN
eurjchem-1080	171	44	,	,	PUNCT
eurjchem-1080	171	45	w.	w.	PROPN
eurjchem-1080	171	46	;	;	PUNCT
eurjchem-1080	171	47	meehan	meehan	PROPN
eurjchem-1080	171	48	,	,	PUNCT
eurjchem-1080	171	49	a.	a.	NOUN
eurjchem-1080	171	50	g.	g.	PROPN
eurjchem-1080	171	51	;	;	PUNCT
eurjchem-1080	171	52	lasseter	lasseter	PROPN
eurjchem-1080	171	53	,	,	PUNCT
eurjchem-1080	171	54	k.	k.	PROPN
eurjchem-1080	171	55	;	;	PUNCT
eurjchem-1080	171	56	dilzer	dilzer	NOUN
eurjchem-1080	171	57	,	,	PUNCT
eurjchem-1080	171	58	s.	s.	PROPN
eurjchem-1080	171	59	;	;	PUNCT
eurjchem-1080	171	60	blum	blum	PROPN
eurjchem-1080	171	61	,	,	PUNCT
eurjchem-1080	171	62	r.	r.	PROPN
eurjchem-1080	171	63	;	;	PUNCT
eurjchem-1080	171	64	wagner	wagner	PROPN
eurjchem-1080	171	65	,	,	PUNCT
eurjchem-1080	171	66	j.	j.	PROPN
eurjchem-1080	171	67	a.	a.	PROPN
eurjchem-1080	171	68	j.	j.	PROPN
eurjchem-1080	171	69	clin	clin	PROPN
eurjchem-1080	171	70	.	.	PUNCT
eurjchem-1080	172	1	pharmacol	pharmacol	PROPN
eurjchem-1080	172	2	.	.	PUNCT
eurjchem-1080	173	1	2006	2006	NUM
eurjchem-1080	173	2	,	,	PUNCT
eurjchem-1080	173	3	46	46	NUM
eurjchem-1080	173	4	,	,	PUNCT
eurjchem-1080	173	5	876‐886	876‐886	NUM
eurjchem-1080	173	6	.	.	PUNCT
eurjchem-1080	174	1	[	[	X
eurjchem-1080	174	2	5	5	NUM
eurjchem-1080	174	3	]	]	PUNCT
eurjchem-1080	174	4	.	.	PUNCT
eurjchem-1080	174	5	eligar	eligar	NOUN
eurjchem-1080	174	6	,	,	PUNCT
eurjchem-1080	174	7	v.	v.	CCONJ
eurjchem-1080	174	8	s.	s.	PROPN
eurjchem-1080	174	9	;	;	PUNCT
eurjchem-1080	174	10	bain	bain	PROPN
eurjchem-1080	174	11	,	,	PUNCT
eurjchem-1080	174	12	s.	s.	PROPN
eurjchem-1080	174	13	c.	c.	PROPN
eurjchem-1080	174	14	drug	drug	PROPN
eurjchem-1080	174	15	des	des	PROPN
eurjchem-1080	174	16	.	.	PROPN
eurjchem-1080	174	17	dev	dev	PROPN
eurjchem-1080	174	18	.	.	PUNCT
eurjchem-1080	175	1	ther	ther	PROPN
eurjchem-1080	175	2	.	.	PUNCT
eurjchem-1080	176	1	2013	2013	NUM
eurjchem-1080	176	2	,	,	PUNCT
eurjchem-1080	176	3	7	7	NUM
eurjchem-1080	176	4	,	,	PUNCT
eurjchem-1080	176	5	893‐903	893‐903	NOUN
eurjchem-1080	176	6	.	.	PUNCT
eurjchem-1080	177	1	[	[	X
eurjchem-1080	177	2	6	6	NUM
eurjchem-1080	177	3	]	]	PUNCT
eurjchem-1080	177	4	.	.	PUNCT
eurjchem-1080	178	1	vincent	vincent	PROPN
eurjchem-1080	178	2	,	,	PUNCT
eurjchem-1080	178	3	s.	s.	PROPN
eurjchem-1080	178	4	h.	h.	PROPN
eurjchem-1080	178	5	;	;	PUNCT
eurjchem-1080	178	6	reed	reed	PROPN
eurjchem-1080	178	7	,	,	PUNCT
eurjchem-1080	178	8	j.	j.	PROPN
eurjchem-1080	178	9	r.	r.	PROPN
eurjchem-1080	178	10	;	;	PUNCT
eurjchem-1080	178	11	bergman	bergman	PROPN
eurjchem-1080	178	12	,	,	PUNCT
eurjchem-1080	178	13	a.	a.	PROPN
eurjchem-1080	178	14	j.	j.	PROPN
eurjchem-1080	178	15	;	;	PUNCT
eurjchem-1080	178	16	elmore	elmore	NOUN
eurjchem-1080	178	17	,	,	PUNCT
eurjchem-1080	178	18	c.	c.	PROPN
eurjchem-1080	178	19	s.	s.	PROPN
eurjchem-1080	178	20	;	;	PUNCT
eurjchem-1080	178	21	zhu	zhu	PROPN
eurjchem-1080	178	22	,	,	PUNCT
eurjchem-1080	178	23	b.	b.	PROPN
eurjchem-1080	178	24	;	;	PUNCT
eurjchem-1080	178	25	xu	xu	PROPN
eurjchem-1080	178	26	,	,	PUNCT
eurjchem-1080	178	27	s.	s.	PROPN
eurjchem-1080	178	28	;	;	PUNCT
eurjchem-1080	178	29	ebel	ebel	PROPN
eurjchem-1080	178	30	,	,	PUNCT
eurjchem-1080	178	31	d.	d.	PROPN
eurjchem-1080	178	32	;	;	PUNCT
eurjchem-1080	178	33	larson	larson	PROPN
eurjchem-1080	178	34	,	,	PUNCT
eurjchem-1080	178	35	p.	p.	PROPN
eurjchem-1080	178	36	;	;	PUNCT
eurjchem-1080	178	37	zeng	zeng	PROPN
eurjchem-1080	178	38	,	,	PUNCT
eurjchem-1080	178	39	w.	w.	PROPN
eurjchem-1080	178	40	;	;	PUNCT
eurjchem-1080	178	41	chen	chen	PROPN
eurjchem-1080	178	42	,	,	PUNCT
eurjchem-1080	178	43	l.	l.	PROPN
eurjchem-1080	178	44	;	;	PUNCT
eurjchem-1080	178	45	dilzer	dilzer	NOUN
eurjchem-1080	178	46	,	,	PUNCT
eurjchem-1080	178	47	s.	s.	PROPN
eurjchem-1080	178	48	;	;	PUNCT
eurjchem-1080	178	49	lasseter	lasseter	PROPN
eurjchem-1080	178	50	,	,	PUNCT
eurjchem-1080	178	51	k.	k.	PROPN
eurjchem-1080	178	52	;	;	PUNCT
eurjchem-1080	178	53	gottesdiener	gottesdiener	PROPN
eurjchem-1080	178	54	,	,	PUNCT
eurjchem-1080	178	55	k.	k.	PROPN
eurjchem-1080	178	56	;	;	PUNCT
eurjchem-1080	178	57	wagner	wagner	PROPN
eurjchem-1080	178	58	,	,	PUNCT
eurjchem-1080	178	59	j.	j.	PROPN
eurjchem-1080	178	60	a.	a.	PROPN
eurjchem-1080	178	61	;	;	PUNCT
eurjchem-1080	178	62	herman	herman	PROPN
eurjchem-1080	178	63	,	,	PUNCT
eurjchem-1080	178	64	g.	g.	PROPN
eurjchem-1080	178	65	a.	a.	PROPN
eurjchem-1080	178	66	drug	drug	PROPN
eurjchem-1080	178	67	metab	metab	PROPN
eurjchem-1080	178	68	.	.	PUNCT
eurjchem-1080	179	1	dispos	dispos	PROPN
eurjchem-1080	179	2	.	.	PUNCT
eurjchem-1080	180	1	2007	2007	NUM
eurjchem-1080	180	2	,	,	PUNCT
eurjchem-1080	180	3	35	35	NUM
eurjchem-1080	180	4	,	,	PUNCT
eurjchem-1080	180	5	533‐538	533‐538	NUM
eurjchem-1080	180	6	.	.	PUNCT
eurjchem-1080	181	1	[	[	X
eurjchem-1080	181	2	7	7	NUM
eurjchem-1080	181	3	]	]	PUNCT
eurjchem-1080	181	4	.	.	PUNCT
eurjchem-1080	182	1	wei	wei	PROPN
eurjchem-1080	182	2	,	,	PUNCT
eurjchem-1080	182	3	z.	z.	PROPN
eurjchem-1080	182	4	;	;	PUNCT
eurjchem-1080	182	5	donald	donald	PROPN
eurjchem-1080	182	6	,	,	PUNCT
eurjchem-1080	182	7	g.	g.	PROPN
eurjchem-1080	182	8	m.	m.	PROPN
eurjchem-1080	182	9	;	;	PUNCT
eurjchem-1080	182	10	alison	alison	PROPN
eurjchem-1080	182	11	,	,	PUNCT
eurjchem-1080	182	12	l.	l.	PROPN
eurjchem-1080	182	13	f.	f.	PROPN
eurjchem-1080	182	14	;	;	PUNCT
eurjchem-1080	182	15	li	li	PROPN
eurjchem-1080	182	16	,	,	PUNCT
eurjchem-1080	182	17	c.	c.	PROPN
eurjchem-1080	182	18	;	;	PUNCT
eurjchem-1080	182	19	michael	michael	PROPN
eurjchem-1080	182	20	,	,	PUNCT
eurjchem-1080	182	21	s.	s.	PROPN
eurjchem-1080	182	22	s.	s.	PROPN
eurjchem-1080	182	23	;	;	PUNCT
eurjchem-1080	182	24	eric	eric	PROPN
eurjchem-1080	182	25	,	,	PUNCT
eurjchem-1080	182	26	j.	j.	PROPN
eurjchem-1080	182	27	w.	w.	PROPN
eurjchem-1080	182	28	;	;	PUNCT
eurjchem-1080	182	29	amy	amy	PROPN
eurjchem-1080	182	30	,	,	PUNCT
eurjchem-1080	182	31	q.	q.	PROPN
eurjchem-1080	182	32	w.	w.	PROPN
eurjchem-1080	182	33	j.	j.	PROPN
eurjchem-1080	182	34	pharmaceut	pharmaceut	PROPN
eurjchem-1080	182	35	.	.	PROPN
eurjchem-1080	182	36	biomed	biome	VERB
eurjchem-1080	182	37	.	.	PUNCT
eurjchem-1080	183	1	2008	2008	NUM
eurjchem-1080	183	2	,	,	PUNCT
eurjchem-1080	183	3	46	46	NUM
eurjchem-1080	183	4	,	,	PUNCT
eurjchem-1080	183	5	534‐542	534‐542	NUM
eurjchem-1080	183	6	.	.	PUNCT
eurjchem-1080	184	1	[	[	X
eurjchem-1080	184	2	8	8	NUM
eurjchem-1080	184	3	]	]	PUNCT
eurjchem-1080	184	4	.	.	PUNCT
eurjchem-1080	185	1	ramakrishna	ramakrishna	PROPN
eurjchem-1080	185	2	,	,	PUNCT
eurjchem-1080	185	3	n.	n.	NOUN
eurjchem-1080	185	4	;	;	PUNCT
eurjchem-1080	185	5	vishwottam	vishwottam	PROPN
eurjchem-1080	185	6	,	,	PUNCT
eurjchem-1080	185	7	k.	k.	PROPN
eurjchem-1080	185	8	;	;	PUNCT
eurjchem-1080	185	9	koteshwara	koteshwara	PROPN
eurjchem-1080	185	10	,	,	PUNCT
eurjchem-1080	185	11	m.	m.	NOUN
eurjchem-1080	185	12	;	;	PUNCT
eurjchem-1080	185	13	prashanth	prashanth	PROPN
eurjchem-1080	185	14	,	,	PUNCT
eurjchem-1080	185	15	k.	k.	PROPN
eurjchem-1080	185	16	;	;	PUNCT
eurjchem-1080	185	17	raghupathi	raghupathi	NOUN
eurjchem-1080	185	18	,	,	PUNCT
eurjchem-1080	185	19	a.	a.	NOUN
eurjchem-1080	185	20	;	;	PUNCT
eurjchem-1080	185	21	rajeshkumar	rajeshkumar	PROPN
eurjchem-1080	185	22	,	,	PUNCT
eurjchem-1080	185	23	b.	b.	PROPN
eurjchem-1080	185	24	biomed	biome	VERB
eurjchem-1080	185	25	.	.	PUNCT
eurjchem-1080	186	1	chromatogr	chromatogr	PROPN
eurjchem-1080	186	2	.	.	PUNCT
eurjchem-1080	187	1	2008	2008	NUM
eurjchem-1080	187	2	,	,	PUNCT
eurjchem-1080	187	3	22	22	NUM
eurjchem-1080	187	4	,	,	PUNCT
eurjchem-1080	187	5	214‐	214‐	NUM
eurjchem-1080	187	6	222	222	NUM
eurjchem-1080	187	7	.	.	PUNCT
eurjchem-1080	188	1	[	[	X
eurjchem-1080	188	2	9	9	NUM
eurjchem-1080	188	3	]	]	PUNCT
eurjchem-1080	188	4	.	.	PUNCT
eurjchem-1080	188	5	beconi	beconi	NOUN
eurjchem-1080	188	6	,	,	PUNCT
eurjchem-1080	188	7	m.	m.	NOUN
eurjchem-1080	188	8	g.	g.	PROPN
eurjchem-1080	188	9	;	;	PUNCT
eurjchem-1080	188	10	reed	reed	PROPN
eurjchem-1080	188	11	,	,	PUNCT
eurjchem-1080	188	12	j.	j.	PROPN
eurjchem-1080	188	13	r.	r.	PROPN
eurjchem-1080	188	14	;	;	PUNCT
eurjchem-1080	188	15	teffera	teffera	NOUN
eurjchem-1080	188	16	,	,	PUNCT
eurjchem-1080	188	17	y.	y.	PROPN
eurjchem-1080	188	18	;	;	PUNCT
eurjchem-1080	188	19	xia	xia	PROPN
eurjchem-1080	188	20	,	,	PUNCT
eurjchem-1080	188	21	y.	y.	PROPN
eurjchem-1080	188	22	q.	q.	PROPN
eurjchem-1080	188	23	;	;	PUNCT
eurjchem-1080	188	24	kochansky	kochansky	PROPN
eurjchem-1080	188	25	,	,	PUNCT
eurjchem-1080	188	26	c.	c.	PROPN
eurjchem-1080	188	27	j.	j.	PROPN
eurjchem-1080	188	28	;	;	PUNCT
eurjchem-1080	188	29	liu	liu	PROPN
eurjchem-1080	188	30	,	,	PUNCT
eurjchem-1080	188	31	d.	d.	PROPN
eurjchem-1080	188	32	q.	q.	PROPN
eurjchem-1080	188	33	;	;	PUNCT
eurjchem-1080	188	34	xu	xu	PROPN
eurjchem-1080	188	35	,	,	PUNCT
eurjchem-1080	188	36	s.	s.	PROPN
eurjchem-1080	188	37	;	;	PUNCT
eurjchem-1080	188	38	elmore	elmore	NOUN
eurjchem-1080	188	39	,	,	PUNCT
eurjchem-1080	188	40	c.	c.	PROPN
eurjchem-1080	188	41	s.	s.	PROPN
eurjchem-1080	188	42	;	;	PUNCT
eurjchem-1080	188	43	ciccotto	ciccotto	PROPN
eurjchem-1080	188	44	,	,	PUNCT
eurjchem-1080	188	45	s.	s.	PROPN
eurjchem-1080	188	46	;	;	PUNCT
eurjchem-1080	188	47	hora	hora	PROPN
eurjchem-1080	188	48	,	,	PUNCT
eurjchem-1080	188	49	d.	d.	PROPN
eurjchem-1080	188	50	f.	f.	PROPN
eurjchem-1080	188	51	;	;	PUNCT
eurjchem-1080	188	52	stearns	stearns	PROPN
eurjchem-1080	188	53	,	,	PUNCT
eurjchem-1080	188	54	r.	r.	PROPN
eurjchem-1080	188	55	a.	a.	PROPN
eurjchem-1080	188	56	;	;	PUNCT
eurjchem-1080	188	57	vincent	vincent	PROPN
eurjchem-1080	188	58	,	,	PUNCT
eurjchem-1080	188	59	s.	s.	PROPN
eurjchem-1080	188	60	h.	h.	PROPN
eurjchem-1080	188	61	drug	drug	PROPN
eurjchem-1080	188	62	metab	metab	PROPN
eurjchem-1080	188	63	.	.	PUNCT
eurjchem-1080	189	1	dispos	dispos	PROPN
eurjchem-1080	189	2	.	.	PUNCT
eurjchem-1080	190	1	2007	2007	NUM
eurjchem-1080	190	2	,	,	PUNCT
eurjchem-1080	190	3	35	35	NUM
eurjchem-1080	190	4	,	,	PUNCT
eurjchem-1080	190	5	525‐532	525‐532	NUM
eurjchem-1080	190	6	.	.	PUNCT
eurjchem-1080	191	1	502	502	NUM
eurjchem-1080	191	2	saleh	saleh	NOUN
eurjchem-1080	191	3	et	et	PROPN
eurjchem-1080	191	4	al	al	PROPN
eurjchem-1080	191	5	.	.	PUNCT
eurjchem-1080	191	6	/	/	SYM
eurjchem-1080	191	7	european	european	PROPN
eurjchem-1080	191	8	journal	journal	PROPN
eurjchem-1080	191	9	of	of	ADP
eurjchem-1080	191	10	chemistry	chemistry	NOUN
eurjchem-1080	191	11	5	5	NUM
eurjchem-1080	191	12	(	(	PUNCT
eurjchem-1080	191	13	3	3	NUM
eurjchem-1080	191	14	)	)	PUNCT
eurjchem-1080	191	15	(	(	PUNCT
eurjchem-1080	191	16	2014	2014	NUM
eurjchem-1080	191	17	)	)	PUNCT
eurjchem-1080	191	18	497‐502	497‐502	NOUN
eurjchem-1080	192	1	[	[	X
eurjchem-1080	192	2	10	10	NUM
eurjchem-1080	192	3	]	]	PUNCT
eurjchem-1080	192	4	.	.	PUNCT
eurjchem-1080	193	1	sekaran	sekaran	NOUN
eurjchem-1080	193	2	,	,	PUNCT
eurjchem-1080	193	3	c.	c.	PROPN
eurjchem-1080	193	4	b.	b.	PROPN
eurjchem-1080	193	5	;	;	PUNCT
eurjchem-1080	193	6	prameela	prameela	PROPN
eurjchem-1080	193	7	,	,	PUNCT
eurjchem-1080	193	8	r.	r.	PROPN
eurjchem-1080	193	9	int	int	PROPN
eurjchem-1080	193	10	.	.	PUNCT
eurjchem-1080	194	1	j.	j.	PROPN
eurjchem-1080	194	2	pharm	pharm	PROPN
eurjchem-1080	194	3	.	.	PUNCT
eurjchem-1080	195	1	pharm	pharm	PROPN
eurjchem-1080	195	2	.	.	PUNCT
eurjchem-1080	196	1	sci	sci	PROPN
eurjchem-1080	196	2	.	.	PROPN
eurjchem-1080	196	3	2010	2010	NUM
eurjchem-1080	196	4	,	,	PUNCT
eurjchem-1080	196	5	2	2	NUM
eurjchem-1080	196	6	,	,	PUNCT
eurjchem-1080	196	7	138‐142	138‐142	NUM
eurjchem-1080	196	8	.	.	PUNCT
eurjchem-1080	197	1	[	[	X
eurjchem-1080	197	2	11	11	NUM
eurjchem-1080	197	3	]	]	PUNCT
eurjchem-1080	197	4	.	.	PUNCT
eurjchem-1080	198	1	raja	raja	PROPN
eurjchem-1080	198	2	,	,	PUNCT
eurjchem-1080	198	3	t.	t.	PROPN
eurjchem-1080	198	4	;	;	PUNCT
eurjchem-1080	198	5	rao	rao	PROPN
eurjchem-1080	198	6	,	,	PUNCT
eurjchem-1080	198	7	a.	a.	PROPN
eurjchem-1080	198	8	l.	l.	PROPN
eurjchem-1080	198	9	int	int	PROPN
eurjchem-1080	198	10	.	.	PUNCT
eurjchem-1080	199	1	j.	j.	PROPN
eurjchem-1080	199	2	pharm	pharm	PROPN
eurjchem-1080	199	3	.	.	PUNCT
eurjchem-1080	200	1	chem	chem	PROPN
eurjchem-1080	200	2	.	.	PUNCT
eurjchem-1080	201	1	biol	biol	PROPN
eurjchem-1080	201	2	.	.	PUNCT
eurjchem-1080	202	1	sci	sci	PROPN
eurjchem-1080	202	2	.	.	PROPN
eurjchem-1080	202	3	2012	2012	NUM
eurjchem-1080	202	4	,	,	PUNCT
eurjchem-1080	202	5	2	2	NUM
eurjchem-1080	202	6	,	,	PUNCT
eurjchem-1080	202	7	696‐702	696‐702	NUM
eurjchem-1080	202	8	.	.	PUNCT
eurjchem-1080	203	1	[	[	X
eurjchem-1080	203	2	12	12	NUM
eurjchem-1080	203	3	]	]	PUNCT
eurjchem-1080	203	4	.	.	PUNCT
eurjchem-1080	204	1	maste	maste	PROPN
eurjchem-1080	204	2	,	,	PUNCT
eurjchem-1080	204	3	m.	m.	NOUN
eurjchem-1080	204	4	m.	m.	NOUN
eurjchem-1080	204	5	;	;	PUNCT
eurjchem-1080	204	6	parate	parate	NOUN
eurjchem-1080	204	7	,	,	PUNCT
eurjchem-1080	204	8	a.	a.	NOUN
eurjchem-1080	204	9	n.	n.	PROPN
eurjchem-1080	204	10	;	;	PUNCT
eurjchem-1080	204	11	bhat	bhat	PROPN
eurjchem-1080	204	12	,	,	PUNCT
eurjchem-1080	204	13	a.	a.	PROPN
eurjchem-1080	204	14	r.	r.	PROPN
eurjchem-1080	204	15	asian	asian	PROPN
eurjchem-1080	204	16	j.	j.	PROPN
eurjchem-1080	204	17	res	res	PROPN
eurjchem-1080	204	18	.	.	PROPN
eurjchem-1080	204	19	chem	chem	PROPN
eurjchem-1080	204	20	.	.	PUNCT
eurjchem-1080	205	1	2011	2011	NUM
eurjchem-1080	205	2	,	,	PUNCT
eurjchem-1080	205	3	4	4	NUM
eurjchem-1080	205	4	,	,	PUNCT
eurjchem-1080	205	5	1466‐1468	1466‐1468	NUM
eurjchem-1080	205	6	.	.	PUNCT
eurjchem-1080	206	1	[	[	X
eurjchem-1080	206	2	13	13	NUM
eurjchem-1080	206	3	]	]	PUNCT
eurjchem-1080	206	4	.	.	PUNCT
eurjchem-1080	207	1	lavanya	lavanya	PROPN
eurjchem-1080	207	2	,	,	PUNCT
eurjchem-1080	207	3	r.	r.	PROPN
eurjchem-1080	207	4	;	;	PUNCT
eurjchem-1080	208	1	yunoos	yunoos	PROPN
eurjchem-1080	208	2	,	,	PUNCT
eurjchem-1080	208	3	md	md	PROPN
eurjchem-1080	208	4	.	.	PUNCT
eurjchem-1080	208	5	j.	j.	PROPN
eurjchem-1080	208	6	adv	adv	PROPN
eurjchem-1080	208	7	.	.	PUNCT
eurjchem-1080	209	1	pharm	pharm	PROPN
eurjchem-1080	209	2	.	.	PUNCT
eurjchem-1080	210	1	edu	edu	PROPN
eurjchem-1080	210	2	.	.	PUNCT
eurjchem-1080	211	1	res	res	PROPN
eurjchem-1080	211	2	.	.	PROPN
eurjchem-1080	212	1	2013	2013	NUM
eurjchem-1080	212	2	,	,	PUNCT
eurjchem-1080	212	3	3	3	NUM
eurjchem-1080	212	4	,	,	PUNCT
eurjchem-1080	212	5	475‐479	475‐479	PROPN
eurjchem-1080	212	6	.	.	PUNCT
eurjchem-1080	213	1	[	[	X
eurjchem-1080	213	2	14	14	NUM
eurjchem-1080	213	3	]	]	SYM
eurjchem-1080	213	4	.	.	PUNCT
eurjchem-1080	214	1	pathan	pathan	PROPN
eurjchem-1080	214	2	,	,	PUNCT
eurjchem-1080	214	3	h.	h.	PROPN
eurjchem-1080	214	4	;	;	PUNCT
eurjchem-1080	214	5	sreenivas	sreenivas	PROPN
eurjchem-1080	214	6	,	,	PUNCT
eurjchem-1080	214	7	r.	r.	PROPN
eurjchem-1080	214	8	t.	t.	PROPN
eurjchem-1080	214	9	;	;	PUNCT
eurjchem-1080	214	10	chandanam	chandanam	PROPN
eurjchem-1080	214	11	,	,	PUNCT
eurjchem-1080	214	12	s.	s.	PROPN
eurjchem-1080	214	13	;	;	PUNCT
eurjchem-1080	214	14	ashok	ashok	PROPN
eurjchem-1080	214	15	,	,	PUNCT
eurjchem-1080	214	16	r.	r.	PROPN
eurjchem-1080	214	17	;	;	PUNCT
eurjchem-1080	214	18	swetha	swetha	PROPN
eurjchem-1080	214	19	,	,	PUNCT
eurjchem-1080	214	20	k.	k.	PROPN
eurjchem-1080	214	21	dhr	dhr	PROPN
eurjchem-1080	214	22	int	int	PROPN
eurjchem-1080	214	23	.	.	PUNCT
eurjchem-1080	215	1	pharm	pharm	PROPN
eurjchem-1080	215	2	.	.	PUNCT
eurjchem-1080	216	1	sci	sci	PROPN
eurjchem-1080	216	2	.	.	PROPN
eurjchem-1080	216	3	2014	2014	NUM
eurjchem-1080	216	4	,	,	PUNCT
eurjchem-1080	216	5	5	5	NUM
eurjchem-1080	216	6	,	,	PUNCT
eurjchem-1080	216	7	80‐87	80‐87	NOUN
eurjchem-1080	216	8	.	.	PUNCT
eurjchem-1080	217	1	[	[	X
eurjchem-1080	217	2	15	15	NUM
eurjchem-1080	217	3	]	]	PUNCT
eurjchem-1080	217	4	.	.	PUNCT
eurjchem-1080	218	1	moffat	moffat	PROPN
eurjchem-1080	218	2	,	,	PUNCT
eurjchem-1080	218	3	a.	a.	PROPN
eurjchem-1080	218	4	c.	c.	PROPN
eurjchem-1080	218	5	;	;	PUNCT
eurjchem-1080	218	6	osselten	osselten	VERB
eurjchem-1080	218	7	,	,	PUNCT
eurjchem-1080	218	8	m.	m.	NOUN
eurjchem-1080	218	9	d.	d.	PROPN
eurjchem-1080	218	10	;	;	PUNCT
eurjchem-1080	218	11	widdop	widdop	PROPN
eurjchem-1080	218	12	,	,	PUNCT
eurjchem-1080	218	13	b.	b.	PROPN
eurjchem-1080	218	14	clarke	clarke	PROPN
eurjchem-1080	218	15	’s	’s	PART
eurjchem-1080	218	16	analysis	analysis	NOUN
eurjchem-1080	218	17	of	of	ADP
eurjchem-1080	218	18	drugs	drug	NOUN
eurjchem-1080	218	19	and	and	CCONJ
eurjchem-1080	218	20	poisons	poison	NOUN
eurjchem-1080	218	21	in	in	ADP
eurjchem-1080	218	22	pharmaceuticals	pharmaceutical	NOUN
eurjchem-1080	218	23	,	,	PUNCT
eurjchem-1080	218	24	body	body	NOUN
eurjchem-1080	218	25	fluids	fluid	NOUN
eurjchem-1080	218	26	and	and	CCONJ
eurjchem-1080	218	27	post	post	NOUN
eurjchem-1080	218	28	mortem	mortem	X
eurjchem-1080	218	29	material	material	NOUN
eurjchem-1080	218	30	,	,	PUNCT
eurjchem-1080	218	31	3rd	3rd	ADJ
eurjchem-1080	218	32	edn	edn	NOUN
eurjchem-1080	218	33	.	.	PUNCT
eurjchem-1080	218	34	,	,	PUNCT
eurjchem-1080	218	35	pharmaceuticals	pharmaceuticals	PROPN
eurjchem-1080	218	36	press	press	PROPN
eurjchem-1080	218	37	:	:	PUNCT
eurjchem-1080	218	38	london	london	PROPN
eurjchem-1080	218	39	,	,	PUNCT
eurjchem-1080	218	40	2004	2004	NUM
eurjchem-1080	218	41	.	.	PUNCT
eurjchem-1080	219	1	[	[	X
eurjchem-1080	219	2	16	16	NUM
eurjchem-1080	219	3	]	]	PUNCT
eurjchem-1080	219	4	.	.	PUNCT
eurjchem-1080	220	1	clark	clark	PROPN
eurjchem-1080	220	2	,	,	PUNCT
eurjchem-1080	220	3	e.	e.	PROPN
eurjchem-1080	220	4	g.	g.	PROPN
eurjchem-1080	220	5	c.	c.	PROPN
eurjchem-1080	220	6	clarke	clarke	PROPN
eurjchem-1080	220	7	’s	’s	PART
eurjchem-1080	220	8	isolation	isolation	NOUN
eurjchem-1080	220	9	and	and	CCONJ
eurjchem-1080	220	10	identification	identification	NOUN
eurjchem-1080	220	11	of	of	ADP
eurjchem-1080	220	12	drugs	drug	NOUN
eurjchem-1080	220	13	in	in	ADP
eurjchem-1080	220	14	pharmaceuticals	pharmaceutical	NOUN
eurjchem-1080	220	15	body	body	NOUN
eurjchem-1080	220	16	fluids	fluid	NOUN
eurjchem-1080	220	17	and	and	CCONJ
eurjchem-1080	220	18	post‐mortem	post‐mortem	NOUN
eurjchem-1080	220	19	materials	material	NOUN
eurjchem-1080	220	20	,	,	PUNCT
eurjchem-1080	220	21	2nd	2nd	ADJ
eurjchem-1080	220	22	edn	edn	NOUN
eurjchem-1080	220	23	.	.	PUNCT
eurjchem-1080	221	1	the	the	DET
eurjchem-1080	221	2	pharmaceutical	pharmaceutical	PROPN
eurjchem-1080	221	3	press	press	NOUN
eurjchem-1080	221	4	:	:	PUNCT
eurjchem-1080	221	5	london	london	PROPN
eurjchem-1080	221	6	,	,	PUNCT
eurjchem-1080	221	7	1986	1986	NUM
eurjchem-1080	221	8	.	.	PUNCT
eurjchem-1080	222	1	[	[	X
eurjchem-1080	222	2	17	17	NUM
eurjchem-1080	222	3	]	]	PUNCT
eurjchem-1080	222	4	.	.	PUNCT
eurjchem-1080	223	1	hinchen	hinchen	PROPN
eurjchem-1080	223	2	,	,	PUNCT
eurjchem-1080	223	3	j.	j.	PROPN
eurjchem-1080	223	4	d.	d.	PROPN
eurjchem-1080	223	5	practical	practical	ADJ
eurjchem-1080	223	6	statistics	statistic	NOUN
eurjchem-1080	223	7	for	for	ADP
eurjchem-1080	223	8	chemical	chemical	NOUN
eurjchem-1080	223	9	research	research	NOUN
eurjchem-1080	223	10	,	,	PUNCT
eurjchem-1080	223	11	1st	1st	ADJ
eurjchem-1080	223	12	edn	edn	PROPN
eurjchem-1080	223	13	.	.	PUNCT
eurjchem-1080	224	1	methuen	methuen	PROPN
eurjchem-1080	224	2	and	and	CCONJ
eurjchem-1080	224	3	science	science	NOUN
eurjchem-1080	224	4	paperbacks	paperback	NOUN
eurjchem-1080	224	5	,	,	PUNCT
eurjchem-1080	224	6	london	london	PROPN
eurjchem-1080	224	7	,	,	PUNCT
eurjchem-1080	224	8	1969	1969	NUM
eurjchem-1080	224	9	.	.	PUNCT