id	sid	tid	token	lemma	pos
eurjchem-1090	1	1	untitled	untitle	VERB
eurjchem-1090	1	2	european	european	PROPN
eurjchem-1090	1	3	journal	journal	PROPN
eurjchem-1090	1	4	of	of	ADP
eurjchem-1090	1	5	chemistry	chemistry	NOUN
eurjchem-1090	1	6	5	5	NUM
eurjchem-1090	1	7	(	(	PUNCT
eurjchem-1090	1	8	4	4	NUM
eurjchem-1090	1	9	)	)	PUNCT
eurjchem-1090	1	10	(	(	PUNCT
eurjchem-1090	1	11	2014	2014	NUM
eurjchem-1090	1	12	)	)	PUNCT
eurjchem-1090	1	13	662‐667	662‐667	NUM
eurjchem-1090	1	14	european	european	ADJ
eurjchem-1090	1	15	journal	journal	NOUN
eurjchem-1090	1	16	of	of	ADP
eurjchem-1090	1	17	chemistry	chemistry	NOUN
eurjchem-1090	1	18	issn	issn	PROPN
eurjchem-1090	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-1090	1	20	(	(	PUNCT
eurjchem-1090	1	21	print	print	NOUN
eurjchem-1090	1	22	)	)	PUNCT
eurjchem-1090	1	23	/	/	SYM
eurjchem-1090	1	24	issn	issn	PROPN
eurjchem-1090	1	25	2153‐2257	2153‐2257	NUM
eurjchem-1090	1	26	(	(	PUNCT
eurjchem-1090	1	27	online	online	ADJ
eurjchem-1090	1	28	)	)	PUNCT
eurjchem-1090	1	29			NOUN
eurjchem-1090	1	30	2014	2014	NUM
eurjchem-1090	2	1	eurjchem	eurjchem	PROPN
eurjchem-1090	2	2	publishing	publish	VERB
eurjchem-1090	2	3	‐	‐	NOUN
eurjchem-1090	2	4	printed	print	VERB
eurjchem-1090	2	5	in	in	ADP
eurjchem-1090	2	6	the	the	DET
eurjchem-1090	2	7	usa	usa	PROPN
eurjchem-1090	2	8	http://dx.doi.org/10.5155/eurjchem.5.4.662‐667.1090	http://dx.doi.org/10.5155/eurjchem.5.4.662‐667.1090	PROPN
eurjchem-1090	2	9	european	european	PROPN
eurjchem-1090	2	10	journal	journal	PROPN
eurjchem-1090	2	11	of	of	ADP
eurjchem-1090	2	12	chemistry	chemistry	PROPN
eurjchem-1090	2	13	journal	journal	PROPN
eurjchem-1090	2	14	homepage	homepage	NOUN
eurjchem-1090	2	15	:	:	PUNCT
eurjchem-1090	2	16	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1090	3	1	liquid	liquid	ADJ
eurjchem-1090	3	2	chromatography‐electro	chromatography‐electro	NOUN
eurjchem-1090	3	3	spray	spray	NOUN
eurjchem-1090	3	4	ionization	ionization	NOUN
eurjchem-1090	3	5	tandem	tandem	NOUN
eurjchem-1090	3	6	mass	mass	ADJ
eurjchem-1090	3	7	spectrometry	spectrometry	NOUN
eurjchem-1090	3	8	for	for	ADP
eurjchem-1090	3	9	simultaneous	simultaneous	ADJ
eurjchem-1090	3	10	determination	determination	NOUN
eurjchem-1090	3	11	of	of	ADP
eurjchem-1090	3	12	moexipril	moexipril	NOUN
eurjchem-1090	3	13	and	and	CCONJ
eurjchem-1090	3	14	its	its	PRON
eurjchem-1090	3	15	active	active	ADJ
eurjchem-1090	3	16	metabolite	metabolite	NOUN
eurjchem-1090	3	17	moexiprilat	moexiprilat	NOUN
eurjchem-1090	3	18	in	in	ADP
eurjchem-1090	3	19	human	human	ADJ
eurjchem-1090	3	20	plasma	plasma	NOUN
eurjchem-1090	3	21	omar	omar	PROPN
eurjchem-1090	3	22	abd	abd	PROPN
eurjchem-1090	3	23	elaziz	elaziz	PROPN
eurjchem-1090	3	24	a	a	PROPN
eurjchem-1090	3	25	,	,	PUNCT
eurjchem-1090	3	26	maha	maha	PROPN
eurjchem-1090	3	27	farouk	farouk	PROPN
eurjchem-1090	3	28	a	a	PROPN
eurjchem-1090	3	29	,	,	PUNCT
eurjchem-1090	3	30	shereen	shereen	NUM
eurjchem-1090	3	31	tawakkol	tawakkol	PROPN
eurjchem-1090	3	32	b	b	PROPN
eurjchem-1090	3	33	,	,	PUNCT
eurjchem-1090	3	34	ahmed	ahmed	PROPN
eurjchem-1090	3	35	hemdan	hemdan	PROPN
eurjchem-1090	3	36	c	c	PROPN
eurjchem-1090	3	37	,	,	PUNCT
eurjchem-1090	3	38	*	*	PUNCT
eurjchem-1090	3	39	and	and	CCONJ
eurjchem-1090	3	40	mostafa	mostafa	PROPN
eurjchem-1090	3	41	shehata	shehata	PROPN
eurjchem-1090	4	1	d	d	PROPN
eurjchem-1090	4	2	a	a	DET
eurjchem-1090	4	3	pharmaceutical	pharmaceutical	ADJ
eurjchem-1090	4	4	analytical	analytical	ADJ
eurjchem-1090	4	5	chemistry	chemistry	NOUN
eurjchem-1090	4	6	department	department	NOUN
eurjchem-1090	4	7	,	,	PUNCT
eurjchem-1090	4	8	faculty	faculty	NOUN
eurjchem-1090	4	9	of	of	ADP
eurjchem-1090	4	10	pharmacy	pharmacy	NOUN
eurjchem-1090	4	11	,	,	PUNCT
eurjchem-1090	4	12	ain	ain	PROPN
eurjchem-1090	4	13	shams	shams	PROPN
eurjchem-1090	4	14	university	university	PROPN
eurjchem-1090	4	15	,	,	PUNCT
eurjchem-1090	4	16	cairo	cairo	PROPN
eurjchem-1090	4	17	,	,	PUNCT
eurjchem-1090	4	18	11566	11566	NUM
eurjchem-1090	4	19	,	,	PUNCT
eurjchem-1090	4	20	egypt	egypt	PROPN
eurjchem-1090	4	21	b	b	PROPN
eurjchem-1090	4	22	pharmaceutical	pharmaceutical	ADJ
eurjchem-1090	4	23	analytical	analytical	ADJ
eurjchem-1090	4	24	chemistry	chemistry	NOUN
eurjchem-1090	4	25	department	department	NOUN
eurjchem-1090	4	26	,	,	PUNCT
eurjchem-1090	4	27	faculty	faculty	NOUN
eurjchem-1090	4	28	of	of	ADP
eurjchem-1090	4	29	pharmacy	pharmacy	NOUN
eurjchem-1090	4	30	,	,	PUNCT
eurjchem-1090	4	31	helwan	helwan	PROPN
eurjchem-1090	4	32	university	university	PROPN
eurjchem-1090	4	33	,	,	PUNCT
eurjchem-1090	4	34	cairo	cairo	PROPN
eurjchem-1090	4	35	,	,	PUNCT
eurjchem-1090	4	36	11431	11431	NUM
eurjchem-1090	4	37	,	,	PUNCT
eurjchem-1090	4	38	egypt	egypt	PROPN
eurjchem-1090	4	39	c	c	PROPN
eurjchem-1090	4	40	pharmaceutical	pharmaceutical	PROPN
eurjchem-1090	4	41	analytical	analytical	ADJ
eurjchem-1090	4	42	chemistry	chemistry	NOUN
eurjchem-1090	4	43	department	department	NOUN
eurjchem-1090	4	44	,	,	PUNCT
eurjchem-1090	4	45	faculty	faculty	NOUN
eurjchem-1090	4	46	of	of	ADP
eurjchem-1090	4	47	pharmacy	pharmacy	NOUN
eurjchem-1090	4	48	,	,	PUNCT
eurjchem-1090	4	49	ahram	ahram	PROPN
eurjchem-1090	4	50	canadian	canadian	PROPN
eurjchem-1090	4	51	university	university	PROPN
eurjchem-1090	4	52	,	,	PUNCT
eurjchem-1090	4	53	6th	6th	NOUN
eurjchem-1090	4	54	of	of	ADP
eurjchem-1090	4	55	october	october	PROPN
eurjchem-1090	4	56	,	,	PUNCT
eurjchem-1090	4	57	12566	12566	NUM
eurjchem-1090	4	58	,	,	PUNCT
eurjchem-1090	4	59	egypt	egypt	PROPN
eurjchem-1090	4	60	d	d	PROPN
eurjchem-1090	4	61	pharmaceutical	pharmaceutical	ADJ
eurjchem-1090	4	62	analytical	analytical	ADJ
eurjchem-1090	4	63	chemistry	chemistry	NOUN
eurjchem-1090	4	64	department	department	NOUN
eurjchem-1090	4	65	,	,	PUNCT
eurjchem-1090	4	66	faculty	faculty	NOUN
eurjchem-1090	4	67	of	of	ADP
eurjchem-1090	4	68	pharmacy	pharmacy	NOUN
eurjchem-1090	4	69	,	,	PUNCT
eurjchem-1090	4	70	cairo	cairo	PROPN
eurjchem-1090	4	71	university	university	PROPN
eurjchem-1090	4	72	,	,	PUNCT
eurjchem-1090	4	73	cairo	cairo	PROPN
eurjchem-1090	4	74	,	,	PUNCT
eurjchem-1090	4	75	12316	12316	NUM
eurjchem-1090	4	76	,	,	PUNCT
eurjchem-1090	4	77	egypt	egypt	PROPN
eurjchem-1090	4	78	*	*	PUNCT
eurjchem-1090	4	79	corresponding	correspond	VERB
eurjchem-1090	4	80	author	author	NOUN
eurjchem-1090	4	81	at	at	ADP
eurjchem-1090	4	82	:	:	PUNCT
eurjchem-1090	4	83	pharmaceutical	pharmaceutical	ADJ
eurjchem-1090	4	84	analytical	analytical	ADJ
eurjchem-1090	4	85	chemistry	chemistry	NOUN
eurjchem-1090	4	86	department	department	NOUN
eurjchem-1090	4	87	,	,	PUNCT
eurjchem-1090	4	88	faculty	faculty	NOUN
eurjchem-1090	4	89	of	of	ADP
eurjchem-1090	4	90	pharmacy	pharmacy	NOUN
eurjchem-1090	4	91	,	,	PUNCT
eurjchem-1090	4	92	ahram	ahram	PROPN
eurjchem-1090	4	93	canadian	canadian	PROPN
eurjchem-1090	4	94	university	university	PROPN
eurjchem-1090	4	95	,	,	PUNCT
eurjchem-1090	4	96	6th	6th	NOUN
eurjchem-1090	4	97	of	of	ADP
eurjchem-1090	4	98	october	october	PROPN
eurjchem-1090	4	99	,	,	PUNCT
eurjchem-1090	4	100	12566	12566	NUM
eurjchem-1090	4	101	,	,	PUNCT
eurjchem-1090	4	102	egypt	egypt	PROPN
eurjchem-1090	4	103	.	.	PUNCT
eurjchem-1090	5	1	tel	tel	PROPN
eurjchem-1090	5	2	.	.	PUNCT
eurjchem-1090	5	3	:	:	PUNCT
eurjchem-1090	6	1	+2.012.21620730	+2.012.21620730	X
eurjchem-1090	6	2	.	.	PUNCT
eurjchem-1090	7	1	fax	fax	NOUN
eurjchem-1090	7	2	:	:	PUNCT
eurjchem-1090	7	3	+2.023.8334379	+2.023.8334379	ADJ
eurjchem-1090	7	4	.	.	PUNCT
eurjchem-1090	7	5	e‐mail	e‐mail	PUNCT
eurjchem-1090	8	1	address	address	NOUN
eurjchem-1090	8	2	:	:	PUNCT
eurjchem-1090	8	3	hemmdan@yahoo.com	hemmdan@yahoo.com	PROPN
eurjchem-1090	8	4	(	(	PUNCT
eurjchem-1090	8	5	a.	a.	PROPN
eurjchem-1090	8	6	hemdan	hemdan	PROPN
eurjchem-1090	8	7	)	)	PUNCT
eurjchem-1090	8	8	.	.	PUNCT
eurjchem-1090	9	1	article	article	NOUN
eurjchem-1090	9	2	information	information	PROPN
eurjchem-1090	9	3	abstract	abstract	ADJ
eurjchem-1090	9	4	doi	doi	NOUN
eurjchem-1090	9	5	:	:	PUNCT
eurjchem-1090	9	6	10.5155	10.5155	NUM
eurjchem-1090	9	7	/	/	SYM
eurjchem-1090	9	8	eurjchem.5.4.662‐667.1090	eurjchem.5.4.662‐667.1090	PRON
eurjchem-1090	9	9	received	receive	VERB
eurjchem-1090	9	10	:	:	PUNCT
eurjchem-1090	9	11	09	09	NUM
eurjchem-1090	9	12	may	may	AUX
eurjchem-1090	9	13	2014	2014	NUM
eurjchem-1090	9	14	received	receive	VERB
eurjchem-1090	9	15	in	in	ADP
eurjchem-1090	9	16	revised	revise	VERB
eurjchem-1090	9	17	form	form	NOUN
eurjchem-1090	9	18	:	:	PUNCT
eurjchem-1090	9	19	04	04	NUM
eurjchem-1090	9	20	july	july	PROPN
eurjchem-1090	9	21	2014	2014	NUM
eurjchem-1090	9	22	accepted	accept	VERB
eurjchem-1090	9	23	:	:	PUNCT
eurjchem-1090	9	24	24	24	NUM
eurjchem-1090	9	25	august	august	PROPN
eurjchem-1090	9	26	2014	2014	NUM
eurjchem-1090	9	27	online	online	NOUN
eurjchem-1090	9	28	:	:	PUNCT
eurjchem-1090	9	29	31	31	NUM
eurjchem-1090	9	30	december	december	PROPN
eurjchem-1090	9	31	2014	2014	NUM
eurjchem-1090	9	32	keywords	keyword	VERB
eurjchem-1090	9	33	a	a	DET
eurjchem-1090	9	34	selective	selective	ADJ
eurjchem-1090	9	35	,	,	PUNCT
eurjchem-1090	9	36	sensitive	sensitive	ADJ
eurjchem-1090	9	37	,	,	PUNCT
eurjchem-1090	9	38	and	and	CCONJ
eurjchem-1090	9	39	rapid	rapid	ADJ
eurjchem-1090	9	40	liquid	liquid	NOUN
eurjchem-1090	9	41	chromatography‐electro	chromatography‐electro	NOUN
eurjchem-1090	9	42	spray	spray	NOUN
eurjchem-1090	9	43	ionization	ionization	NOUN
eurjchem-1090	9	44	tandem	tandem	PROPN
eurjchem-1090	9	45	mass	mass	PROPN
eurjchem-1090	9	46	spectrometry	spectrometry	NOUN
eurjchem-1090	9	47	method	method	NOUN
eurjchem-1090	9	48	has	have	AUX
eurjchem-1090	9	49	been	be	AUX
eurjchem-1090	9	50	developed	develop	VERB
eurjchem-1090	9	51	and	and	CCONJ
eurjchem-1090	9	52	subsequently	subsequently	ADV
eurjchem-1090	9	53	validated	validate	VERB
eurjchem-1090	9	54	for	for	ADP
eurjchem-1090	9	55	the	the	DET
eurjchem-1090	9	56	simultaneous	simultaneous	ADJ
eurjchem-1090	9	57	determination	determination	NOUN
eurjchem-1090	9	58	of	of	ADP
eurjchem-1090	9	59	moexipril	moexipril	NOUN
eurjchem-1090	9	60	(	(	PUNCT
eurjchem-1090	9	61	mox	mox	NOUN
eurjchem-1090	9	62	)	)	PUNCT
eurjchem-1090	9	63	,	,	PUNCT
eurjchem-1090	9	64	and	and	CCONJ
eurjchem-1090	9	65	its	its	PRON
eurjchem-1090	9	66	active	active	ADJ
eurjchem-1090	9	67	metabolite	metabolite	NOUN
eurjchem-1090	9	68	moexiprilat	moexiprilat	NOUN
eurjchem-1090	9	69	(	(	PUNCT
eurjchem-1090	9	70	moxt	moxt	NOUN
eurjchem-1090	9	71	)	)	PUNCT
eurjchem-1090	9	72	in	in	ADP
eurjchem-1090	9	73	spiked	spiked	ADJ
eurjchem-1090	9	74	human	human	ADJ
eurjchem-1090	9	75	plasma	plasma	NOUN
eurjchem-1090	9	76	,	,	PUNCT
eurjchem-1090	9	77	using	use	VERB
eurjchem-1090	9	78	benazepril	benazepril	PROPN
eurjchem-1090	9	79	(	(	PUNCT
eurjchem-1090	9	80	benz	benz	PROPN
eurjchem-1090	9	81	)	)	PUNCT
eurjchem-1090	9	82	as	as	ADP
eurjchem-1090	9	83	an	an	DET
eurjchem-1090	9	84	internal	internal	ADJ
eurjchem-1090	9	85	standard	standard	NOUN
eurjchem-1090	9	86	(	(	PUNCT
eurjchem-1090	9	87	is	be	AUX
eurjchem-1090	9	88	)	)	PUNCT
eurjchem-1090	9	89	.	.	PUNCT
eurjchem-1090	10	1	various	various	ADJ
eurjchem-1090	10	2	modes	mode	NOUN
eurjchem-1090	10	3	were	be	AUX
eurjchem-1090	10	4	tried	try	VERB
eurjchem-1090	10	5	and	and	CCONJ
eurjchem-1090	10	6	the	the	DET
eurjchem-1090	10	7	multiple	multiple	ADJ
eurjchem-1090	10	8	reaction	reaction	NOUN
eurjchem-1090	10	9	monitoring	monitoring	NOUN
eurjchem-1090	10	10	(	(	PUNCT
eurjchem-1090	10	11	mrm	mrm	PROPN
eurjchem-1090	10	12	)	)	PUNCT
eurjchem-1090	10	13	mode	mode	NOUN
eurjchem-1090	10	14	was	be	AUX
eurjchem-1090	10	15	found	find	VERB
eurjchem-1090	10	16	the	the	DET
eurjchem-1090	10	17	most	most	ADV
eurjchem-1090	10	18	suitable	suitable	ADJ
eurjchem-1090	10	19	one	one	NUM
eurjchem-1090	10	20	.	.	PUNCT
eurjchem-1090	11	1	the	the	DET
eurjchem-1090	11	2	two	two	NUM
eurjchem-1090	11	3	analytes	analyte	NOUN
eurjchem-1090	11	4	and	and	CCONJ
eurjchem-1090	11	5	benazepril	benazepril	ADJ
eurjchem-1090	11	6	(	(	PUNCT
eurjchem-1090	11	7	is	be	AUX
eurjchem-1090	11	8	)	)	PUNCT
eurjchem-1090	11	9	were	be	AUX
eurjchem-1090	11	10	extracted	extract	VERB
eurjchem-1090	11	11	from	from	ADP
eurjchem-1090	11	12	human	human	ADJ
eurjchem-1090	11	13	plasma	plasma	NOUN
eurjchem-1090	11	14	by	by	ADP
eurjchem-1090	11	15	simple	simple	ADJ
eurjchem-1090	11	16	protein	protein	NOUN
eurjchem-1090	11	17	precipitation	precipitation	NOUN
eurjchem-1090	11	18	using	use	VERB
eurjchem-1090	11	19	acetonitrile	acetonitrile	NOUN
eurjchem-1090	11	20	as	as	ADP
eurjchem-1090	11	21	the	the	DET
eurjchem-1090	11	22	precipitating	precipitating	NOUN
eurjchem-1090	11	23	solvent	solvent	NOUN
eurjchem-1090	11	24	.	.	PUNCT
eurjchem-1090	12	1	the	the	DET
eurjchem-1090	12	2	stationary	stationary	ADJ
eurjchem-1090	12	3	phase	phase	NOUN
eurjchem-1090	12	4	used	use	VERB
eurjchem-1090	12	5	was	be	AUX
eurjchem-1090	12	6	a	a	DET
eurjchem-1090	12	7	c18	c18	NOUN
eurjchem-1090	12	8	sunfire	sunfire	NOUN
eurjchem-1090	12	9	column	column	PROPN
eurjchem-1090	12	10	while	while	SCONJ
eurjchem-1090	12	11	water	water	NOUN
eurjchem-1090	12	12	and	and	CCONJ
eurjchem-1090	12	13	acetonitrile	acetonitrile	NOUN
eurjchem-1090	12	14	at	at	ADP
eurjchem-1090	12	15	0.1	0.1	NUM
eurjchem-1090	12	16	%	%	NOUN
eurjchem-1090	12	17	formic	formic	ADJ
eurjchem-1090	12	18	acid	acid	NOUN
eurjchem-1090	12	19	(	(	PUNCT
eurjchem-1090	12	20	30:70	30:70	NUM
eurjchem-1090	12	21	,	,	PUNCT
eurjchem-1090	12	22	v	v	NOUN
eurjchem-1090	12	23	:	:	SYM
eurjchem-1090	12	24	v	v	NOUN
eurjchem-1090	12	25	)	)	PUNCT
eurjchem-1090	12	26	was	be	AUX
eurjchem-1090	12	27	used	use	VERB
eurjchem-1090	12	28	as	as	ADP
eurjchem-1090	12	29	a	a	DET
eurjchem-1090	12	30	mobile	mobile	ADJ
eurjchem-1090	12	31	phase	phase	NOUN
eurjchem-1090	12	32	.	.	PUNCT
eurjchem-1090	13	1	the	the	DET
eurjchem-1090	13	2	flow	flow	NOUN
eurjchem-1090	13	3	rate	rate	NOUN
eurjchem-1090	13	4	used	use	VERB
eurjchem-1090	13	5	was	be	AUX
eurjchem-1090	13	6	0.8	0.8	NUM
eurjchem-1090	13	7	ml	ml	NOUN
eurjchem-1090	13	8	/	/	SYM
eurjchem-1090	13	9	min	min	PROPN
eurjchem-1090	13	10	.	.	PROPN
eurjchem-1090	13	11	food	food	PROPN
eurjchem-1090	13	12	and	and	CCONJ
eurjchem-1090	13	13	drug	drug	PROPN
eurjchem-1090	13	14	administration	administration	NOUN
eurjchem-1090	13	15	guidelines	guideline	NOUN
eurjchem-1090	13	16	were	be	AUX
eurjchem-1090	13	17	followed	follow	VERB
eurjchem-1090	13	18	for	for	ADP
eurjchem-1090	13	19	the	the	DET
eurjchem-1090	13	20	method	method	NOUN
eurjchem-1090	13	21	validation	validation	NOUN
eurjchem-1090	13	22	.	.	PUNCT
eurjchem-1090	14	1	the	the	DET
eurjchem-1090	14	2	linearity	linearity	NOUN
eurjchem-1090	14	3	range	range	NOUN
eurjchem-1090	14	4	was	be	AUX
eurjchem-1090	14	5	found	find	VERB
eurjchem-1090	14	6	to	to	PART
eurjchem-1090	14	7	be	be	AUX
eurjchem-1090	14	8	0.5‐100	0.5‐100	NUM
eurjchem-1090	14	9	ng	ng	PROPN
eurjchem-1090	14	10	/	/	SYM
eurjchem-1090	14	11	ml	ml	X
eurjchem-1090	14	12	for	for	ADP
eurjchem-1090	14	13	mox	mox	NOUN
eurjchem-1090	14	14	and	and	CCONJ
eurjchem-1090	14	15	5‐200	5‐200	PROPN
eurjchem-1090	14	16	ng	ng	PROPN
eurjchem-1090	14	17	/	/	SYM
eurjchem-1090	14	18	ml	ml	X
eurjchem-1090	14	19	for	for	ADP
eurjchem-1090	14	20	moxt	moxt	NOUN
eurjchem-1090	14	21	and	and	CCONJ
eurjchem-1090	14	22	the	the	DET
eurjchem-1090	14	23	correlation	correlation	NOUN
eurjchem-1090	14	24	coefficient	coefficient	NOUN
eurjchem-1090	14	25	was	be	AUX
eurjchem-1090	14	26	more	more	ADJ
eurjchem-1090	14	27	than	than	ADP
eurjchem-1090	14	28	0.9980	0.9980	NUM
eurjchem-1090	14	29	for	for	ADP
eurjchem-1090	14	30	each	each	DET
eurjchem-1090	14	31	analyte	analyte	NOUN
eurjchem-1090	14	32	.	.	PUNCT
eurjchem-1090	15	1	results	result	NOUN
eurjchem-1090	15	2	for	for	ADP
eurjchem-1090	15	3	accuracy	accuracy	NOUN
eurjchem-1090	15	4	and	and	CCONJ
eurjchem-1090	15	5	precision	precision	NOUN
eurjchem-1090	15	6	showed	show	VERB
eurjchem-1090	15	7	satisfactory	satisfactory	ADJ
eurjchem-1090	15	8	results	result	NOUN
eurjchem-1090	15	9	.	.	PUNCT
eurjchem-1090	16	1	also	also	ADV
eurjchem-1090	16	2	the	the	DET
eurjchem-1090	16	3	method	method	NOUN
eurjchem-1090	16	4	was	be	AUX
eurjchem-1090	16	5	compared	compare	VERB
eurjchem-1090	16	6	with	with	ADP
eurjchem-1090	16	7	reported	report	VERB
eurjchem-1090	16	8	hplc	hplc	NOUN
eurjchem-1090	16	9	method	method	NOUN
eurjchem-1090	16	10	and	and	CCONJ
eurjchem-1090	16	11	no	no	DET
eurjchem-1090	16	12	significant	significant	ADJ
eurjchem-1090	16	13	difference	difference	NOUN
eurjchem-1090	16	14	was	be	AUX
eurjchem-1090	16	15	found	find	VERB
eurjchem-1090	16	16	.	.	PUNCT
eurjchem-1090	17	1	plasma	plasma	NOUN
eurjchem-1090	17	2	moexipril	moexipril	PROPN
eurjchem-1090	17	3	lc‐ms	lc‐ms	AUX
eurjchem-1090	17	4	/	/	SYM
eurjchem-1090	17	5	ms	ms	PROPN
eurjchem-1090	17	6	benazepril	benazepril	PROPN
eurjchem-1090	17	7	moexiprilat	moexiprilat	PROPN
eurjchem-1090	17	8	simple	simple	ADJ
eurjchem-1090	17	9	protein	protein	NOUN
eurjchem-1090	17	10	precipitation	precipitation	NOUN
eurjchem-1090	17	11	1	1	NUM
eurjchem-1090	17	12	.	.	PUNCT
eurjchem-1090	18	1	introduction	introduction	NOUN
eurjchem-1090	18	2	moexipril	moexipril	NOUN
eurjchem-1090	18	3	(	(	PUNCT
eurjchem-1090	18	4	3s)‐2‐[(2s)‐2‐[[(1s)‐1‐(ethoxycarbonyl)‐3‐	3s)‐2‐[(2s)‐2‐[[(1s)‐1‐(ethoxycarbonyl)‐3‐	NUM
eurjchem-1090	18	5	phenylpropyl]amino]‐1‐oxopropyl]‐1	phenylpropyl]amino]‐1‐oxopropyl]‐1	NOUN
eurjchem-1090	18	6	,	,	PUNCT
eurjchem-1090	18	7	2	2	NUM
eurjchem-1090	18	8	,	,	PUNCT
eurjchem-1090	18	9	3	3	NUM
eurjchem-1090	18	10	,	,	PUNCT
eurjchem-1090	18	11	4‐tetrahydro‐6	4‐tetrahydro‐6	PROPN
eurjchem-1090	18	12	,	,	PUNCT
eurjchem-1090	18	13	7‐	7‐	NUM
eurjchem-1090	18	14	dimethoxy‐3‐isoquinolinecarboxylic	dimethoxy‐3‐isoquinolinecarboxylic	NOUN
eurjchem-1090	18	15	acid	acid	NOUN
eurjchem-1090	19	1	[	[	X
eurjchem-1090	19	2	1	1	NUM
eurjchem-1090	19	3	]	]	PUNCT
eurjchem-1090	19	4	is	be	AUX
eurjchem-1090	19	5	an	an	DET
eurjchem-1090	19	6	antihyperten‐	antihyperten‐	ADV
eurjchem-1090	19	7	sive	sive	ADJ
eurjchem-1090	19	8	drug	drug	NOUN
eurjchem-1090	19	9	,	,	PUNCT
eurjchem-1090	19	10	which	which	PRON
eurjchem-1090	19	11	belongs	belong	VERB
eurjchem-1090	19	12	to	to	ADP
eurjchem-1090	19	13	the	the	DET
eurjchem-1090	19	14	group	group	NOUN
eurjchem-1090	19	15	of	of	ADP
eurjchem-1090	19	16	angiotensin	angiotensin	NOUN
eurjchem-1090	19	17	convertase	convertase	PROPN
eurjchem-1090	19	18	inhibitors	inhibitor	NOUN
eurjchem-1090	19	19	.	.	PUNCT
eurjchem-1090	20	1	moexipril	moexipril	NOUN
eurjchem-1090	20	2	hydrochloride	hydrochloride	NOUN
eurjchem-1090	20	3	is	be	AUX
eurjchem-1090	20	4	a	a	DET
eurjchem-1090	20	5	long‐acting	long‐acting	NOUN
eurjchem-1090	20	6	non‐	non‐	ADV
eurjchem-1090	20	7	sulfhydryl	sulfhydryl	ADJ
eurjchem-1090	20	8	angiotensin‐converting	angiotensin‐converte	VERB
eurjchem-1090	20	9	enzyme	enzyme	NOUN
eurjchem-1090	20	10	(	(	PUNCT
eurjchem-1090	20	11	ace	ace	NOUN
eurjchem-1090	20	12	)	)	PUNCT
eurjchem-1090	20	13	inhibitor	inhibitor	NOUN
eurjchem-1090	20	14	,	,	PUNCT
eurjchem-1090	20	15	developed	develop	VERB
eurjchem-1090	20	16	for	for	ADP
eurjchem-1090	20	17	the	the	DET
eurjchem-1090	20	18	treatment	treatment	NOUN
eurjchem-1090	20	19	of	of	ADP
eurjchem-1090	20	20	hypertension	hypertension	NOUN
eurjchem-1090	20	21	and	and	CCONJ
eurjchem-1090	20	22	congestive	congestive	ADJ
eurjchem-1090	20	23	heart	heart	NOUN
eurjchem-1090	20	24	failure	failure	NOUN
eurjchem-1090	20	25	.	.	PUNCT
eurjchem-1090	21	1	moexipril	moexipril	NOUN
eurjchem-1090	21	2	is	be	AUX
eurjchem-1090	21	3	a	a	DET
eurjchem-1090	21	4	pro‐drug	pro‐drug	NOUN
eurjchem-1090	21	5	of	of	ADP
eurjchem-1090	21	6	moexiprilat	moexiprilat	NOUN
eurjchem-1090	21	7	,	,	PUNCT
eurjchem-1090	21	8	which	which	PRON
eurjchem-1090	21	9	inhibits	inhibit	VERB
eurjchem-1090	21	10	ace	ace	NOUN
eurjchem-1090	21	11	in	in	ADP
eurjchem-1090	21	12	humans	human	NOUN
eurjchem-1090	21	13	and	and	CCONJ
eurjchem-1090	21	14	animals	animal	NOUN
eurjchem-1090	21	15	.	.	PUNCT
eurjchem-1090	22	1	in	in	ADP
eurjchem-1090	22	2	biological	biological	ADJ
eurjchem-1090	22	3	systems	system	NOUN
eurjchem-1090	22	4	it	it	PRON
eurjchem-1090	22	5	is	be	AUX
eurjchem-1090	22	6	rapidly	rapidly	ADV
eurjchem-1090	22	7	de‐esterified	de‐esterifie	VERB
eurjchem-1090	22	8	by	by	ADP
eurjchem-1090	22	9	esterases	esterase	NOUN
eurjchem-1090	22	10	,	,	PUNCT
eurjchem-1090	22	11	resulting	result	VERB
eurjchem-1090	22	12	in	in	ADP
eurjchem-1090	22	13	its	its	PRON
eurjchem-1090	22	14	active	active	ADJ
eurjchem-1090	22	15	metabolite	metabolite	NOUN
eurjchem-1090	22	16	moexiprilat	moexiprilat	NOUN
eurjchem-1090	23	1	[	[	X
eurjchem-1090	23	2	2,3	2,3	NUM
eurjchem-1090	23	3	]	]	PUNCT
eurjchem-1090	23	4	.	.	PUNCT
eurjchem-1090	24	1	it	it	PRON
eurjchem-1090	24	2	is	be	AUX
eurjchem-1090	24	3	reported	report	VERB
eurjchem-1090	24	4	that	that	SCONJ
eurjchem-1090	24	5	mox	mox	NOUN
eurjchem-1090	24	6	was	be	AUX
eurjchem-1090	24	7	identified	identify	VERB
eurjchem-1090	24	8	by	by	ADP
eurjchem-1090	24	9	hplc	hplc	NOUN
eurjchem-1090	24	10	[	[	X
eurjchem-1090	24	11	4‐6	4‐6	PROPN
eurjchem-1090	24	12	]	]	X
eurjchem-1090	24	13	,	,	PUNCT
eurjchem-1090	24	14	spectrophotometry	spectrophotometry	NOUN
eurjchem-1090	24	15	[	[	X
eurjchem-1090	24	16	7,8	7,8	NUM
eurjchem-1090	24	17	]	]	PUNCT
eurjchem-1090	24	18	,	,	PUNCT
eurjchem-1090	24	19	gas	gas	NOUN
eurjchem-1090	24	20	chromatography	chromatography	NOUN
eurjchem-1090	24	21	mass	mass	PROPN
eurjchem-1090	24	22	spectro‐	spectro‐	PROPN
eurjchem-1090	24	23	metry	metry	NOUN
eurjchem-1090	25	1	[	[	X
eurjchem-1090	25	2	9	9	NUM
eurjchem-1090	25	3	]	]	PUNCT
eurjchem-1090	25	4	,	,	PUNCT
eurjchem-1090	25	5	and	and	CCONJ
eurjchem-1090	25	6	liquid	liquid	ADJ
eurjchem-1090	25	7	chromatography	chromatography	NOUN
eurjchem-1090	25	8	tandem	tandem	PROPN
eurjchem-1090	25	9	mass	mass	PROPN
eurjchem-1090	25	10	spectro‐	spectro‐	PROPN
eurjchem-1090	25	11	metry	metry	NOUN
eurjchem-1090	25	12	[	[	X
eurjchem-1090	25	13	10,11	10,11	NOUN
eurjchem-1090	25	14	]	]	PUNCT
eurjchem-1090	25	15	.	.	PUNCT
eurjchem-1090	26	1	in	in	ADP
eurjchem-1090	26	2	2006	2006	NUM
eurjchem-1090	26	3	,	,	PUNCT
eurjchem-1090	26	4	koti	koti	PROPN
eurjchem-1090	26	5	,	,	PUNCT
eurjchem-1090	26	6	j.	j.	PROPN
eurjchem-1090	26	7	et	et	PROPN
eurjchem-1090	26	8	al	al	PROPN
eurjchem-1090	26	9	.	.	PROPN
eurjchem-1090	26	10	developed	develop	VERB
eurjchem-1090	26	11	a	a	DET
eurjchem-1090	26	12	lc‐mass	lc‐mass	ADJ
eurjchem-1090	26	13	spectrometry	spectrometry	NOUN
eurjchem-1090	26	14	method	method	NOUN
eurjchem-1090	26	15	just	just	ADV
eurjchem-1090	26	16	to	to	PART
eurjchem-1090	26	17	monitor	monitor	VERB
eurjchem-1090	26	18	the	the	DET
eurjchem-1090	26	19	metabolism	metabolism	NOUN
eurjchem-1090	26	20	of	of	ADP
eurjchem-1090	26	21	mox	mox	NOUN
eurjchem-1090	26	22	to	to	PART
eurjchem-1090	26	23	moxt	moxt	VERB
eurjchem-1090	26	24	[	[	X
eurjchem-1090	26	25	10	10	NUM
eurjchem-1090	26	26	]	]	PUNCT
eurjchem-1090	26	27	.	.	PUNCT
eurjchem-1090	27	1	also	also	ADV
eurjchem-1090	27	2	,	,	PUNCT
eurjchem-1090	27	3	in	in	ADP
eurjchem-1090	27	4	2012	2012	NUM
eurjchem-1090	27	5	,	,	PUNCT
eurjchem-1090	27	6	karra	karra	VERB
eurjchem-1090	27	7	et	et	PROPN
eurjchem-1090	27	8	al	al	PROPN
eurjchem-1090	27	9	.	.	PROPN
eurjchem-1090	27	10	developed	develop	VERB
eurjchem-1090	27	11	a	a	DET
eurjchem-1090	27	12	method	method	NOUN
eurjchem-1090	27	13	for	for	ADP
eurjchem-1090	27	14	determination	determination	NOUN
eurjchem-1090	27	15	of	of	ADP
eurjchem-1090	27	16	mox	mox	NOUN
eurjchem-1090	27	17	by	by	ADP
eurjchem-1090	27	18	lc‐tandem	lc‐tandem	PROPN
eurjchem-1090	27	19	mass	mass	PROPN
eurjchem-1090	27	20	spectrometry	spectrometry	NOUN
eurjchem-1090	27	21	.	.	PUNCT
eurjchem-1090	28	1	but	but	CCONJ
eurjchem-1090	28	2	moxt	moxt	NOUN
eurjchem-1090	28	3	,	,	PUNCT
eurjchem-1090	28	4	which	which	PRON
eurjchem-1090	28	5	is	be	AUX
eurjchem-1090	28	6	the	the	DET
eurjchem-1090	28	7	active	active	ADJ
eurjchem-1090	28	8	metabolite	metabolite	NOUN
eurjchem-1090	28	9	was	be	AUX
eurjchem-1090	28	10	not	not	PART
eurjchem-1090	28	11	determined	determine	VERB
eurjchem-1090	28	12	[	[	PUNCT
eurjchem-1090	28	13	11	11	NUM
eurjchem-1090	28	14	]	]	SYM
eurjchem-1090	28	15	.	.	PUNCT
eurjchem-1090	29	1	mox	mox	NOUN
eurjchem-1090	29	2	is	be	AUX
eurjchem-1090	29	3	only	only	ADV
eurjchem-1090	29	4	a	a	DET
eurjchem-1090	29	5	pro‐drug	pro‐drug	NOUN
eurjchem-1090	29	6	,	,	PUNCT
eurjchem-1090	29	7	which	which	PRON
eurjchem-1090	29	8	is	be	AUX
eurjchem-1090	29	9	converted	convert	VERB
eurjchem-1090	29	10	inside	inside	ADP
eurjchem-1090	29	11	the	the	DET
eurjchem-1090	29	12	body	body	NOUN
eurjchem-1090	29	13	to	to	PART
eurjchem-1090	29	14	moxt	moxt	VERB
eurjchem-1090	29	15	,	,	PUNCT
eurjchem-1090	29	16	the	the	DET
eurjchem-1090	29	17	active	active	ADJ
eurjchem-1090	29	18	form	form	NOUN
eurjchem-1090	29	19	.	.	PUNCT
eurjchem-1090	30	1	there	there	PRON
eurjchem-1090	30	2	is	be	VERB
eurjchem-1090	30	3	no	no	DET
eurjchem-1090	30	4	report	report	NOUN
eurjchem-1090	30	5	of	of	ADP
eurjchem-1090	30	6	liquid	liquid	ADJ
eurjchem-1090	30	7	chromatography‐tandem	chromatography‐tandem	PROPN
eurjchem-1090	30	8	mass	mass	PROPN
eurjchem-1090	30	9	spectrometry	spectrometry	NOUN
eurjchem-1090	30	10	studies	study	NOUN
eurjchem-1090	30	11	for	for	ADP
eurjchem-1090	30	12	simultaneous	simultaneous	ADJ
eurjchem-1090	30	13	estimation	estimation	NOUN
eurjchem-1090	30	14	of	of	ADP
eurjchem-1090	30	15	mox	mox	NOUN
eurjchem-1090	30	16	and	and	CCONJ
eurjchem-1090	30	17	its	its	PRON
eurjchem-1090	30	18	active	active	ADJ
eurjchem-1090	30	19	metabolite	metabolite	NOUN
eurjchem-1090	30	20	moxt	moxt	NOUN
eurjchem-1090	30	21	in	in	ADP
eurjchem-1090	30	22	human	human	ADJ
eurjchem-1090	30	23	plasma	plasma	NOUN
eurjchem-1090	30	24	.	.	PUNCT
eurjchem-1090	31	1	this	this	DET
eurjchem-1090	31	2	manuscript	manuscript	NOUN
eurjchem-1090	31	3	presents	present	VERB
eurjchem-1090	31	4	for	for	ADP
eurjchem-1090	31	5	the	the	DET
eurjchem-1090	31	6	first	first	ADJ
eurjchem-1090	31	7	time	time	NOUN
eurjchem-1090	31	8	the	the	DET
eurjchem-1090	31	9	develop‐	develop‐	NOUN
eurjchem-1090	31	10	ment	ment	NOUN
eurjchem-1090	31	11	and	and	CCONJ
eurjchem-1090	31	12	validation	validation	NOUN
eurjchem-1090	31	13	of	of	ADP
eurjchem-1090	31	14	a	a	DET
eurjchem-1090	31	15	sensitive	sensitive	ADJ
eurjchem-1090	31	16	,	,	PUNCT
eurjchem-1090	31	17	selective	selective	ADJ
eurjchem-1090	31	18	and	and	CCONJ
eurjchem-1090	31	19	specific	specific	ADJ
eurjchem-1090	31	20	lc‐	lc‐	ADJ
eurjchem-1090	31	21	ms	ms	PROPN
eurjchem-1090	31	22	/	/	SYM
eurjchem-1090	31	23	ms	ms	PROPN
eurjchem-1090	31	24	method	method	NOUN
eurjchem-1090	31	25	in	in	ADP
eurjchem-1090	31	26	multiple	multiple	ADJ
eurjchem-1090	31	27	reactions	reaction	NOUN
eurjchem-1090	31	28	monitoring	monitor	VERB
eurjchem-1090	31	29	(	(	PUNCT
eurjchem-1090	31	30	mrm	mrm	PROPN
eurjchem-1090	31	31	)	)	PUNCT
eurjchem-1090	31	32	mode	mode	NOUN
eurjchem-1090	31	33	for	for	ADP
eurjchem-1090	31	34	the	the	DET
eurjchem-1090	31	35	quantification	quantification	NOUN
eurjchem-1090	31	36	of	of	ADP
eurjchem-1090	31	37	mox	mox	NOUN
eurjchem-1090	31	38	and	and	CCONJ
eurjchem-1090	31	39	moxt	moxt	NOUN
eurjchem-1090	31	40	in	in	ADP
eurjchem-1090	31	41	human	human	ADJ
eurjchem-1090	31	42	plasma	plasma	NOUN
eurjchem-1090	31	43	using	use	VERB
eurjchem-1090	31	44	benazepril	benazepril	PROPN
eurjchem-1090	31	45	(	(	PUNCT
eurjchem-1090	31	46	benz	benz	PROPN
eurjchem-1090	31	47	)	)	PUNCT
eurjchem-1090	31	48	as	as	ADP
eurjchem-1090	31	49	an	an	DET
eurjchem-1090	31	50	internal	internal	ADJ
eurjchem-1090	31	51	standard	standard	NOUN
eurjchem-1090	31	52	(	(	PUNCT
eurjchem-1090	31	53	is	be	AUX
eurjchem-1090	31	54	)	)	PUNCT
eurjchem-1090	31	55	.	.	PUNCT
eurjchem-1090	32	1	2	2	X
eurjchem-1090	32	2	.	.	X
eurjchem-1090	32	3	experimental	experimental	ADJ
eurjchem-1090	32	4	2.1	2.1	NUM
eurjchem-1090	32	5	.	.	PUNCT
eurjchem-1090	33	1	materials	material	NOUN
eurjchem-1090	33	2	and	and	CCONJ
eurjchem-1090	33	3	reagents	reagent	NOUN
eurjchem-1090	33	4	mox	mox	NOUN
eurjchem-1090	33	5	and	and	CCONJ
eurjchem-1090	33	6	benz	benz	PROPN
eurjchem-1090	33	7	were	be	AUX
eurjchem-1090	33	8	kindly	kindly	ADV
eurjchem-1090	33	9	supplied	supply	VERB
eurjchem-1090	33	10	from	from	ADP
eurjchem-1090	33	11	national	national	ADJ
eurjchem-1090	33	12	organization	organization	NOUN
eurjchem-1090	33	13	for	for	ADP
eurjchem-1090	33	14	drug	drug	NOUN
eurjchem-1090	33	15	control	control	NOUN
eurjchem-1090	33	16	and	and	CCONJ
eurjchem-1090	33	17	research	research	NOUN
eurjchem-1090	33	18	(	(	PUNCT
eurjchem-1090	33	19	nodcar	nodcar	PROPN
eurjchem-1090	33	20	,	,	PUNCT
eurjchem-1090	33	21	cairo	cairo	PROPN
eurjchem-1090	33	22	,	,	PUNCT
eurjchem-1090	33	23	egypt	egypt	PROPN
eurjchem-1090	33	24	)	)	PUNCT
eurjchem-1090	33	25	.	.	PUNCT
eurjchem-1090	34	1	the	the	DET
eurjchem-1090	34	2	purity	purity	NOUN
eurjchem-1090	34	3	of	of	ADP
eurjchem-1090	34	4	the	the	DET
eurjchem-1090	34	5	standards	standard	NOUN
eurjchem-1090	34	6	was	be	AUX
eurjchem-1090	34	7	higher	high	ADJ
eurjchem-1090	34	8	than	than	ADP
eurjchem-1090	34	9	99	99	NUM
eurjchem-1090	34	10	%	%	NOUN
eurjchem-1090	34	11	.	.	PUNCT
eurjchem-1090	35	1	where	where	SCONJ
eurjchem-1090	35	2	moxt	moxt	NOUN
eurjchem-1090	35	3	was	be	AUX
eurjchem-1090	35	4	prepared	prepare	VERB
eurjchem-1090	35	5	by	by	ADP
eurjchem-1090	35	6	the	the	DET
eurjchem-1090	35	7	basic	basic	ADJ
eurjchem-1090	35	8	hydrolysis	hydrolysis	NOUN
eurjchem-1090	35	9	of	of	ADP
eurjchem-1090	35	10	mox	mox	NOUN
eurjchem-1090	35	11	as	as	SCONJ
eurjchem-1090	35	12	will	will	AUX
eurjchem-1090	35	13	be	be	AUX
eurjchem-1090	35	14	explained	explain	VERB
eurjchem-1090	35	15	in	in	ADP
eurjchem-1090	35	16	section	section	NOUN
eurjchem-1090	35	17	2.5.1	2.5.1	NUM
eurjchem-1090	35	18	.	.	PUNCT
eurjchem-1090	36	1	structures	structure	NOUN
eurjchem-1090	36	2	of	of	ADP
eurjchem-1090	36	3	the	the	DET
eurjchem-1090	36	4	compounds	compound	NOUN
eurjchem-1090	36	5	are	be	AUX
eurjchem-1090	36	6	shown	show	VERB
eurjchem-1090	36	7	in	in	ADP
eurjchem-1090	36	8	figure	figure	NOUN
eurjchem-1090	36	9	1	1	NUM
eurjchem-1090	36	10	.	.	PUNCT
eurjchem-1090	37	1	elaziz	elaziz	PROPN
eurjchem-1090	37	2	et	et	PROPN
eurjchem-1090	37	3	al	al	PROPN
eurjchem-1090	37	4	.	.	PUNCT
eurjchem-1090	37	5	/	/	SYM
eurjchem-1090	37	6	european	european	PROPN
eurjchem-1090	37	7	journal	journal	PROPN
eurjchem-1090	37	8	of	of	ADP
eurjchem-1090	37	9	chemistry	chemistry	NOUN
eurjchem-1090	37	10	5	5	NUM
eurjchem-1090	37	11	(	(	PUNCT
eurjchem-1090	37	12	4	4	NUM
eurjchem-1090	37	13	)	)	PUNCT
eurjchem-1090	37	14	(	(	PUNCT
eurjchem-1090	37	15	2014	2014	NUM
eurjchem-1090	37	16	)	)	PUNCT
eurjchem-1090	37	17	662‐667	662‐667	NUM
eurjchem-1090	37	18	663	663	NUM
eurjchem-1090	37	19	(	(	PUNCT
eurjchem-1090	37	20	a	a	NOUN
eurjchem-1090	37	21	)	)	PUNCT
eurjchem-1090	37	22	(	(	PUNCT
eurjchem-1090	37	23	b	b	X
eurjchem-1090	37	24	)	)	PUNCT
eurjchem-1090	37	25	(	(	PUNCT
eurjchem-1090	37	26	c	c	X
eurjchem-1090	37	27	)	)	PUNCT
eurjchem-1090	37	28	figure	figure	NOUN
eurjchem-1090	37	29	1	1	NUM
eurjchem-1090	37	30	.	.	PUNCT
eurjchem-1090	38	1	chemical	chemical	ADJ
eurjchem-1090	38	2	structure	structure	NOUN
eurjchem-1090	38	3	of	of	ADP
eurjchem-1090	38	4	(	(	PUNCT
eurjchem-1090	38	5	a	a	PRON
eurjchem-1090	38	6	)	)	PUNCT
eurjchem-1090	38	7	moexipril	moexipril	NOUN
eurjchem-1090	38	8	,	,	PUNCT
eurjchem-1090	38	9	(	(	PUNCT
eurjchem-1090	38	10	b	b	NOUN
eurjchem-1090	38	11	)	)	PUNCT
eurjchem-1090	38	12	moexiprilat	moexiprilat	NOUN
eurjchem-1090	38	13	,	,	PUNCT
eurjchem-1090	38	14	and	and	CCONJ
eurjchem-1090	38	15	(	(	PUNCT
eurjchem-1090	38	16	c	c	X
eurjchem-1090	38	17	)	)	PUNCT
eurjchem-1090	38	18	benazepril	benazepril	NOUN
eurjchem-1090	38	19	.	.	PUNCT
eurjchem-1090	39	1	hplc‐grade	hplc‐grade	PROPN
eurjchem-1090	39	2	acetonitrile	acetonitrile	NOUN
eurjchem-1090	39	3	(	(	PUNCT
eurjchem-1090	39	4	sigma‐aldrich	sigma‐aldrich	NOUN
eurjchem-1090	39	5	)	)	PUNCT
eurjchem-1090	39	6	,	,	PUNCT
eurjchem-1090	39	7	and	and	CCONJ
eurjchem-1090	39	8	ultrapure	ultrapure	NOUN
eurjchem-1090	39	9	water	water	NOUN
eurjchem-1090	39	10	prepared	prepare	VERB
eurjchem-1090	39	11	by	by	ADP
eurjchem-1090	39	12	a	a	DET
eurjchem-1090	39	13	millipore	millipore	PROPN
eurjchem-1090	39	14	milli‐q	milli‐q	PROPN
eurjchem-1090	39	15	purification	purification	NOUN
eurjchem-1090	39	16	system	system	NOUN
eurjchem-1090	39	17	(	(	PUNCT
eurjchem-1090	39	18	millipore	millipore	PROPN
eurjchem-1090	39	19	corp	corp	PROPN
eurjchem-1090	39	20	.	.	PROPN
eurjchem-1090	39	21	bedford	bedford	PROPN
eurjchem-1090	39	22	,	,	PUNCT
eurjchem-1090	39	23	ma	ma	PROPN
eurjchem-1090	39	24	,	,	PUNCT
eurjchem-1090	39	25	usa	usa	PROPN
eurjchem-1090	39	26	)	)	PUNCT
eurjchem-1090	39	27	were	be	AUX
eurjchem-1090	39	28	used	use	VERB
eurjchem-1090	39	29	as	as	ADP
eurjchem-1090	39	30	mobile	mobile	ADJ
eurjchem-1090	39	31	phase	phase	NOUN
eurjchem-1090	39	32	of	of	ADP
eurjchem-1090	39	33	the	the	DET
eurjchem-1090	39	34	hplc‐ms‐ms	hplc‐ms‐ms	NOUN
eurjchem-1090	39	35	.	.	PUNCT
eurjchem-1090	40	1	other	other	ADJ
eurjchem-1090	40	2	reagents	reagent	NOUN
eurjchem-1090	40	3	were	be	AUX
eurjchem-1090	40	4	of	of	ADP
eurjchem-1090	40	5	analytical‐grade	analytical‐grade	NOUN
eurjchem-1090	40	6	.	.	PUNCT
eurjchem-1090	41	1	drug‐free	drug‐free	PROPN
eurjchem-1090	41	2	human	human	ADJ
eurjchem-1090	41	3	plasma	plasma	NOUN
eurjchem-1090	41	4	was	be	AUX
eurjchem-1090	41	5	obtained	obtain	VERB
eurjchem-1090	41	6	from	from	ADP
eurjchem-1090	41	7	the	the	DET
eurjchem-1090	41	8	holding	hold	VERB
eurjchem-1090	41	9	company	company	NOUN
eurjchem-1090	41	10	for	for	ADP
eurjchem-1090	41	11	biological	biological	ADJ
eurjchem-1090	41	12	products	product	NOUN
eurjchem-1090	41	13	&	&	CCONJ
eurjchem-1090	41	14	vaccines	vaccine	NOUN
eurjchem-1090	41	15	(	(	PUNCT
eurjchem-1090	41	16	vacsera	vacsera	PROPN
eurjchem-1090	41	17	,	,	PUNCT
eurjchem-1090	41	18	cairo	cairo	PROPN
eurjchem-1090	41	19	,	,	PUNCT
eurjchem-1090	41	20	egypt	egypt	PROPN
eurjchem-1090	41	21	)	)	PUNCT
eurjchem-1090	41	22	.	.	PUNCT
eurjchem-1090	42	1	plasma	plasma	NOUN
eurjchem-1090	42	2	was	be	AUX
eurjchem-1090	42	3	stored	store	VERB
eurjchem-1090	42	4	below	below	ADP
eurjchem-1090	42	5	‐40	‐40	PROPN
eurjchem-1090	42	6	°	°	NOUN
eurjchem-1090	42	7	c	c	NOUN
eurjchem-1090	42	8	until	until	SCONJ
eurjchem-1090	42	9	used	use	VERB
eurjchem-1090	42	10	for	for	ADP
eurjchem-1090	42	11	analysis	analysis	NOUN
eurjchem-1090	42	12	.	.	PUNCT
eurjchem-1090	43	1	2.2	2.2	NUM
eurjchem-1090	43	2	.	.	PUNCT
eurjchem-1090	44	1	instruments	instrument	NOUN
eurjchem-1090	44	2	analysis	analysis	NOUN
eurjchem-1090	44	3	was	be	AUX
eurjchem-1090	44	4	performed	perform	VERB
eurjchem-1090	44	5	on	on	ADP
eurjchem-1090	44	6	a	a	DET
eurjchem-1090	44	7	chromatographic	chromatographic	ADJ
eurjchem-1090	44	8	system	system	NOUN
eurjchem-1090	44	9	shimadzu	shimadzu	ADJ
eurjchem-1090	44	10	lc‐20	lc‐20	PROPN
eurjchem-1090	44	11	at	at	ADP
eurjchem-1090	44	12	series	series	NOUN
eurjchem-1090	44	13	hplc	hplc	NOUN
eurjchem-1090	44	14	system	system	NOUN
eurjchem-1090	44	15	(	(	PUNCT
eurjchem-1090	44	16	japan	japan	PROPN
eurjchem-1090	44	17	)	)	PUNCT
eurjchem-1090	44	18	equipped	equip	VERB
eurjchem-1090	44	19	with	with	ADP
eurjchem-1090	44	20	lc‐20	lc‐20	PROPN
eurjchem-1090	44	21	at	at	ADP
eurjchem-1090	44	22	hplc	hplc	NOUN
eurjchem-1090	44	23	pump	pump	NOUN
eurjchem-1090	44	24	,	,	PUNCT
eurjchem-1090	44	25	shimadzu	shimadzu	PROPN
eurjchem-1090	44	26	series	series	PROPN
eurjchem-1090	44	27	dgu‐20a5	dgu‐20a5	PROPN
eurjchem-1090	44	28	degasser	degasser	PROPN
eurjchem-1090	44	29	and	and	CCONJ
eurjchem-1090	44	30	a	a	DET
eurjchem-1090	44	31	shimadzu	shimadzu	ADJ
eurjchem-1090	44	32	sil‐20a	sil‐20a	NOUN
eurjchem-1090	44	33	auto	auto	NOUN
eurjchem-1090	44	34	sampler	sampler	NOUN
eurjchem-1090	44	35	.	.	PUNCT
eurjchem-1090	45	1	a	a	DET
eurjchem-1090	45	2	chromatographic	chromatographic	ADJ
eurjchem-1090	45	3	separation	separation	NOUN
eurjchem-1090	45	4	was	be	AUX
eurjchem-1090	45	5	achieved	achieve	VERB
eurjchem-1090	45	6	by	by	ADP
eurjchem-1090	45	7	a	a	DET
eurjchem-1090	45	8	sunfire	sunfire	NOUN
eurjchem-1090	45	9	c18	c18	NOUN
eurjchem-1090	45	10	column	column	NOUN
eurjchem-1090	45	11	(	(	PUNCT
eurjchem-1090	45	12	50×4.6	50×4.6	PROPN
eurjchem-1090	45	13	mm	mm	NOUN
eurjchem-1090	45	14	,	,	PUNCT
eurjchem-1090	45	15	5	5	NUM
eurjchem-1090	45	16	µm	µm	NOUN
eurjchem-1090	45	17	,	,	PUNCT
eurjchem-1090	45	18	waters	water	NOUN
eurjchem-1090	45	19	,	,	PUNCT
eurjchem-1090	45	20	usa	usa	PROPN
eurjchem-1090	45	21	)	)	PUNCT
eurjchem-1090	45	22	and	and	CCONJ
eurjchem-1090	45	23	a	a	DET
eurjchem-1090	45	24	mixture	mixture	NOUN
eurjchem-1090	45	25	of	of	ADP
eurjchem-1090	45	26	0.1	0.1	NUM
eurjchem-1090	45	27	%	%	NOUN
eurjchem-1090	45	28	formic	formic	ADJ
eurjchem-1090	45	29	acid	acid	NOUN
eurjchem-1090	45	30	:	:	PUNCT
eurjchem-1090	45	31	acetonitrile	acetonitrile	NOUN
eurjchem-1090	45	32	(	(	PUNCT
eurjchem-1090	45	33	30:70	30:70	NUM
eurjchem-1090	45	34	,	,	PUNCT
eurjchem-1090	45	35	v	v	NOUN
eurjchem-1090	45	36	:	:	SYM
eurjchem-1090	45	37	v	v	NOUN
eurjchem-1090	45	38	)	)	PUNCT
eurjchem-1090	45	39	as	as	ADP
eurjchem-1090	45	40	a	a	DET
eurjchem-1090	45	41	mobile	mobile	ADJ
eurjchem-1090	45	42	phase	phase	NOUN
eurjchem-1090	45	43	.	.	PUNCT
eurjchem-1090	46	1	the	the	DET
eurjchem-1090	46	2	isocratic	isocratic	ADJ
eurjchem-1090	46	3	mobile	mobile	ADJ
eurjchem-1090	46	4	phase	phase	NOUN
eurjchem-1090	46	5	,	,	PUNCT
eurjchem-1090	46	6	was	be	AUX
eurjchem-1090	46	7	filtered	filter	VERB
eurjchem-1090	46	8	through	through	ADP
eurjchem-1090	46	9	a	a	DET
eurjchem-1090	46	10	0.45	0.45	NUM
eurjchem-1090	46	11	µm	µm	ADP
eurjchem-1090	46	12	membrane	membrane	NOUN
eurjchem-1090	46	13	filter	filter	NOUN
eurjchem-1090	46	14	(	(	PUNCT
eurjchem-1090	46	15	millipore	millipore	PROPN
eurjchem-1090	46	16	,	,	PUNCT
eurjchem-1090	46	17	usa	usa	PROPN
eurjchem-1090	46	18	)	)	PUNCT
eurjchem-1090	46	19	,	,	PUNCT
eurjchem-1090	46	20	then	then	ADV
eurjchem-1090	46	21	sent	send	VERB
eurjchem-1090	46	22	to	to	ADP
eurjchem-1090	46	23	sonicator	sonicator	VERB
eurjchem-1090	46	24	for	for	ADP
eurjchem-1090	46	25	5	5	NUM
eurjchem-1090	46	26	min	min	NOUN
eurjchem-1090	46	27	.	.	PUNCT
eurjchem-1090	47	1	the	the	DET
eurjchem-1090	47	2	flow	flow	NOUN
eurjchem-1090	47	3	rate	rate	NOUN
eurjchem-1090	47	4	used	use	VERB
eurjchem-1090	47	5	was	be	AUX
eurjchem-1090	47	6	0.8	0.8	NUM
eurjchem-1090	47	7	ml	ml	NOUN
eurjchem-1090	47	8	/	/	SYM
eurjchem-1090	47	9	min	min	NOUN
eurjchem-1090	47	10	.	.	PUNCT
eurjchem-1090	48	1	the	the	DET
eurjchem-1090	48	2	multiple	multiple	ADJ
eurjchem-1090	48	3	reaction	reaction	NOUN
eurjchem-1090	48	4	monitoring	monitoring	NOUN
eurjchem-1090	48	5	(	(	PUNCT
eurjchem-1090	48	6	mrm	mrm	PROPN
eurjchem-1090	48	7	)	)	PUNCT
eurjchem-1090	48	8	in	in	ADP
eurjchem-1090	48	9	positive	positive	ADJ
eurjchem-1090	48	10	ion	ion	NOUN
eurjchem-1090	48	11	mode	mode	NOUN
eurjchem-1090	48	12	was	be	AUX
eurjchem-1090	48	13	used	use	VERB
eurjchem-1090	48	14	for	for	ADP
eurjchem-1090	48	15	quantitative	quantitative	ADJ
eurjchem-1090	48	16	determination	determination	NOUN
eurjchem-1090	48	17	of	of	ADP
eurjchem-1090	48	18	the	the	DET
eurjchem-1090	48	19	analytes	analyte	NOUN
eurjchem-1090	48	20	and	and	CCONJ
eurjchem-1090	48	21	is	be	AUX
eurjchem-1090	48	22	using	use	VERB
eurjchem-1090	48	23	a	a	DET
eurjchem-1090	48	24	mds	mds	NOUN
eurjchem-1090	48	25	sciex	sciex	NOUN
eurjchem-1090	48	26	(	(	PUNCT
eurjchem-1090	48	27	foster	foster	ADJ
eurjchem-1090	48	28	city	city	NOUN
eurjchem-1090	48	29	,	,	PUNCT
eurjchem-1090	48	30	ca	ca	PROPN
eurjchem-1090	48	31	,	,	PUNCT
eurjchem-1090	48	32	usa	usa	PROPN
eurjchem-1090	48	33	)	)	PUNCT
eurjchem-1090	48	34	api‐3200	api‐3200	PROPN
eurjchem-1090	48	35	lc‐	lc‐	ADJ
eurjchem-1090	48	36	ms	ms	PROPN
eurjchem-1090	48	37	/	/	SYM
eurjchem-1090	48	38	ms	ms	PROPN
eurjchem-1090	48	39	triple	triple	ADJ
eurjchem-1090	48	40	quadrupole	quadrupole	PROPN
eurjchem-1090	48	41	mass	mass	NOUN
eurjchem-1090	48	42	spectrometer	spectrometer	NOUN
eurjchem-1090	48	43	,	,	PUNCT
eurjchem-1090	48	44	equipped	equip	VERB
eurjchem-1090	48	45	with	with	ADP
eurjchem-1090	48	46	a	a	DET
eurjchem-1090	48	47	turbo	turbo	NOUN
eurjchem-1090	48	48	ion	ion	NOUN
eurjchem-1090	48	49	spray	spray	NOUN
eurjchem-1090	48	50	interface	interface	NOUN
eurjchem-1090	48	51	at	at	ADP
eurjchem-1090	48	52	350	350	NUM
eurjchem-1090	48	53	°	°	NOUN
eurjchem-1090	48	54	c	c	NOUN
eurjchem-1090	48	55	.	.	PUNCT
eurjchem-1090	49	1	the	the	DET
eurjchem-1090	49	2	common	common	ADJ
eurjchem-1090	49	3	parameters	parameter	NOUN
eurjchem-1090	49	4	,	,	PUNCT
eurjchem-1090	49	5	collision	collision	NOUN
eurjchem-1090	49	6	activated	activate	VERB
eurjchem-1090	49	7	dissociation	dissociation	NOUN
eurjchem-1090	49	8	gas	gas	NOUN
eurjchem-1090	49	9	(	(	PUNCT
eurjchem-1090	49	10	cad	cad	NOUN
eurjchem-1090	49	11	)	)	PUNCT
eurjchem-1090	49	12	,	,	PUNCT
eurjchem-1090	49	13	nebulizer	nebulizer	NOUN
eurjchem-1090	49	14	gas	gas	NOUN
eurjchem-1090	49	15	(	(	PUNCT
eurjchem-1090	49	16	gs1	gs1	NOUN
eurjchem-1090	49	17	)	)	PUNCT
eurjchem-1090	49	18	,	,	PUNCT
eurjchem-1090	49	19	and	and	CCONJ
eurjchem-1090	49	20	heater	heater	NOUN
eurjchem-1090	49	21	gas	gas	NOUN
eurjchem-1090	49	22	(	(	PUNCT
eurjchem-1090	49	23	gs2	gs2	PROPN
eurjchem-1090	49	24	)	)	PUNCT
eurjchem-1090	49	25	were	be	AUX
eurjchem-1090	49	26	set	set	VERB
eurjchem-1090	49	27	at	at	ADP
eurjchem-1090	49	28	5	5	NUM
eurjchem-1090	49	29	,	,	PUNCT
eurjchem-1090	49	30	30	30	NUM
eurjchem-1090	49	31	and	and	CCONJ
eurjchem-1090	49	32	40	40	NUM
eurjchem-1090	49	33	psi	psi	NOUN
eurjchem-1090	49	34	,	,	PUNCT
eurjchem-1090	49	35	respectively	respectively	ADV
eurjchem-1090	49	36	.	.	PUNCT
eurjchem-1090	50	1	the	the	DET
eurjchem-1090	50	2	compound	compound	NOUN
eurjchem-1090	50	3	parameters	parameter	NOUN
eurjchem-1090	50	4	,	,	PUNCT
eurjchem-1090	50	5	collision	collision	NOUN
eurjchem-1090	50	6	exit	exit	NOUN
eurjchem-1090	50	7	potential	potential	NOUN
eurjchem-1090	50	8	(	(	PUNCT
eurjchem-1090	50	9	cxp	cxp	PROPN
eurjchem-1090	50	10	)	)	PUNCT
eurjchem-1090	50	11	,	,	PUNCT
eurjchem-1090	50	12	collision	collision	VERB
eurjchem-1090	50	13	energy	energy	NOUN
eurjchem-1090	50	14	(	(	PUNCT
eurjchem-1090	50	15	ce	ce	PROPN
eurjchem-1090	50	16	)	)	PUNCT
eurjchem-1090	50	17	,	,	PUNCT
eurjchem-1090	50	18	and	and	CCONJ
eurjchem-1090	50	19	declustering	declustere	VERB
eurjchem-1090	50	20	potential	potential	ADJ
eurjchem-1090	50	21	(	(	PUNCT
eurjchem-1090	50	22	dp	dp	NOUN
eurjchem-1090	50	23	)	)	PUNCT
eurjchem-1090	50	24	for	for	ADP
eurjchem-1090	50	25	the	the	DET
eurjchem-1090	50	26	analytes	analyte	NOUN
eurjchem-1090	50	27	and	and	CCONJ
eurjchem-1090	50	28	is	be	AUX
eurjchem-1090	50	29	were	be	AUX
eurjchem-1090	50	30	set	set	VERB
eurjchem-1090	50	31	at	at	ADP
eurjchem-1090	50	32	12	12	NUM
eurjchem-1090	50	33	,	,	PUNCT
eurjchem-1090	50	34	31	31	NUM
eurjchem-1090	50	35	,	,	PUNCT
eurjchem-1090	50	36	and	and	CCONJ
eurjchem-1090	50	37	56	56	NUM
eurjchem-1090	50	38	v	v	NOUN
eurjchem-1090	50	39	,	,	PUNCT
eurjchem-1090	50	40	respectively	respectively	ADV
eurjchem-1090	50	41	.	.	PUNCT
eurjchem-1090	51	1	simultaneous	simultaneous	ADJ
eurjchem-1090	51	2	quantitative	quantitative	ADJ
eurjchem-1090	51	3	determination	determination	NOUN
eurjchem-1090	51	4	of	of	ADP
eurjchem-1090	51	5	mox	mox	NOUN
eurjchem-1090	51	6	,	,	PUNCT
eurjchem-1090	51	7	moxt	moxt	NOUN
eurjchem-1090	51	8	,	,	PUNCT
eurjchem-1090	51	9	and	and	CCONJ
eurjchem-1090	51	10	is	be	AUX
eurjchem-1090	51	11	was	be	AUX
eurjchem-1090	51	12	done	do	VERB
eurjchem-1090	51	13	by	by	ADP
eurjchem-1090	51	14	monitoring	monitor	VERB
eurjchem-1090	51	15	the	the	DET
eurjchem-1090	51	16	parent	parent	NOUN
eurjchem-1090	51	17	/	/	SYM
eurjchem-1090	51	18	daughter	daughter	NOUN
eurjchem-1090	51	19	ions	ion	NOUN
eurjchem-1090	51	20	at	at	ADP
eurjchem-1090	51	21	m	m	PROPN
eurjchem-1090	51	22	/	/	SYM
eurjchem-1090	51	23	z	z	NOUN
eurjchem-1090	51	24	499.4/234.2	499.4/234.2	NOUN
eurjchem-1090	51	25	,	,	PUNCT
eurjchem-1090	51	26	471/206	471/206	NUM
eurjchem-1090	51	27	,	,	PUNCT
eurjchem-1090	51	28	and	and	CCONJ
eurjchem-1090	51	29	425.2/351.2	425.2/351.2	NUM
eurjchem-1090	51	30	,	,	PUNCT
eurjchem-1090	51	31	respectively	respectively	ADV
eurjchem-1090	51	32	.	.	PUNCT
eurjchem-1090	52	1	data	datum	NOUN
eurjchem-1090	52	2	acquisition	acquisition	NOUN
eurjchem-1090	52	3	was	be	AUX
eurjchem-1090	52	4	made	make	VERB
eurjchem-1090	52	5	with	with	ADP
eurjchem-1090	52	6	analyst	analyst	NOUN
eurjchem-1090	52	7	software	software	NOUN
eurjchem-1090	52	8	(	(	PUNCT
eurjchem-1090	52	9	version	version	NOUN
eurjchem-1090	52	10	1.4.2	1.4.2	NUM
eurjchem-1090	52	11	)	)	PUNCT
eurjchem-1090	52	12	.	.	PUNCT
eurjchem-1090	53	1	2.3	2.3	NUM
eurjchem-1090	53	2	.	.	PUNCT
eurjchem-1090	53	3	preparation	preparation	NOUN
eurjchem-1090	53	4	of	of	ADP
eurjchem-1090	53	5	standard	standard	ADJ
eurjchem-1090	53	6	solutions	solution	NOUN
eurjchem-1090	53	7	,	,	PUNCT
eurjchem-1090	53	8	calibration	calibration	NOUN
eurjchem-1090	53	9	standards	standard	NOUN
eurjchem-1090	53	10	and	and	CCONJ
eurjchem-1090	53	11	quality	quality	NOUN
eurjchem-1090	53	12	control	control	NOUN
eurjchem-1090	53	13	samples	sample	VERB
eurjchem-1090	53	14	standard	standard	ADJ
eurjchem-1090	53	15	solutions	solution	NOUN
eurjchem-1090	53	16	of	of	ADP
eurjchem-1090	53	17	mox	mox	NOUN
eurjchem-1090	53	18	,	,	PUNCT
eurjchem-1090	53	19	moxt	moxt	NOUN
eurjchem-1090	53	20	,	,	PUNCT
eurjchem-1090	53	21	and	and	CCONJ
eurjchem-1090	53	22	internal	internal	ADJ
eurjchem-1090	53	23	standard	standard	NOUN
eurjchem-1090	53	24	(	(	PUNCT
eurjchem-1090	53	25	1	1	NUM
eurjchem-1090	53	26	mg	mg	NUM
eurjchem-1090	53	27	/	/	SYM
eurjchem-1090	53	28	ml	ml	NOUN
eurjchem-1090	53	29	)	)	PUNCT
eurjchem-1090	53	30	were	be	AUX
eurjchem-1090	53	31	prepared	prepare	VERB
eurjchem-1090	53	32	in	in	ADP
eurjchem-1090	53	33	acetonitrile	acetonitrile	NOUN
eurjchem-1090	53	34	.	.	PUNCT
eurjchem-1090	54	1	further	further	ADJ
eurjchem-1090	54	2	dilution	dilution	NOUN
eurjchem-1090	54	3	was	be	AUX
eurjchem-1090	54	4	done	do	VERB
eurjchem-1090	54	5	for	for	ADP
eurjchem-1090	54	6	the	the	DET
eurjchem-1090	54	7	preparation	preparation	NOUN
eurjchem-1090	54	8	of	of	ADP
eurjchem-1090	54	9	standard	standard	ADJ
eurjchem-1090	54	10	working	working	ADJ
eurjchem-1090	54	11	solution	solution	NOUN
eurjchem-1090	54	12	of	of	ADP
eurjchem-1090	54	13	mox	mox	NOUN
eurjchem-1090	54	14	,	,	PUNCT
eurjchem-1090	54	15	moxt	moxt	NOUN
eurjchem-1090	54	16	,	,	PUNCT
eurjchem-1090	54	17	and	and	CCONJ
eurjchem-1090	54	18	internal	internal	ADJ
eurjchem-1090	54	19	standard	standard	NOUN
eurjchem-1090	54	20	(	(	PUNCT
eurjchem-1090	54	21	1	1	NUM
eurjchem-1090	54	22	µg	µg	NOUN
eurjchem-1090	54	23	/	/	SYM
eurjchem-1090	54	24	ml	ml	NOUN
eurjchem-1090	54	25	)	)	PUNCT
eurjchem-1090	54	26	.	.	PUNCT
eurjchem-1090	55	1	the	the	DET
eurjchem-1090	55	2	standard	standard	ADJ
eurjchem-1090	55	3	working	work	VERB
eurjchem-1090	55	4	solutions	solution	NOUN
eurjchem-1090	55	5	were	be	AUX
eurjchem-1090	55	6	stored	store	VERB
eurjchem-1090	55	7	at	at	ADP
eurjchem-1090	55	8	4	4	NUM
eurjchem-1090	55	9	°	°	NOUN
eurjchem-1090	55	10	c	c	NOUN
eurjchem-1090	55	11	until	until	SCONJ
eurjchem-1090	55	12	used	use	VERB
eurjchem-1090	55	13	for	for	ADP
eurjchem-1090	55	14	analysis	analysis	NOUN
eurjchem-1090	55	15	,	,	PUNCT
eurjchem-1090	55	16	where	where	SCONJ
eurjchem-1090	55	17	they	they	PRON
eurjchem-1090	55	18	were	be	AUX
eurjchem-1090	55	19	equilibrated	equilibrate	VERB
eurjchem-1090	55	20	to	to	ADP
eurjchem-1090	55	21	room	room	NOUN
eurjchem-1090	55	22	temperature	temperature	NOUN
eurjchem-1090	55	23	.	.	PUNCT
eurjchem-1090	56	1	different	different	ADJ
eurjchem-1090	56	2	aliquots	aliquot	NOUN
eurjchem-1090	56	3	from	from	ADP
eurjchem-1090	56	4	the	the	DET
eurjchem-1090	56	5	standard	standard	ADJ
eurjchem-1090	56	6	working	work	VERB
eurjchem-1090	56	7	solutions	solution	NOUN
eurjchem-1090	56	8	were	be	AUX
eurjchem-1090	56	9	used	use	VERB
eurjchem-1090	56	10	for	for	ADP
eurjchem-1090	56	11	spiking	spike	VERB
eurjchem-1090	56	12	blank	blank	ADJ
eurjchem-1090	56	13	human	human	ADJ
eurjchem-1090	56	14	plasma	plasma	NOUN
eurjchem-1090	56	15	to	to	PART
eurjchem-1090	56	16	prepare	prepare	VERB
eurjchem-1090	56	17	calibration	calibration	NOUN
eurjchem-1090	56	18	standards	standard	NOUN
eurjchem-1090	56	19	and	and	CCONJ
eurjchem-1090	56	20	quality	quality	NOUN
eurjchem-1090	56	21	control	control	NOUN
eurjchem-1090	56	22	samples	sample	NOUN
eurjchem-1090	56	23	.	.	PUNCT
eurjchem-1090	57	1	six	six	NUM
eurjchem-1090	57	2	different	different	ADJ
eurjchem-1090	57	3	concentrations	concentration	NOUN
eurjchem-1090	57	4	of	of	ADP
eurjchem-1090	57	5	mox	mox	NOUN
eurjchem-1090	57	6	(	(	PUNCT
eurjchem-1090	57	7	0.5‐100	0.5‐100	NUM
eurjchem-1090	57	8	ng	ng	PROPN
eurjchem-1090	57	9	/	/	SYM
eurjchem-1090	57	10	ml	ml	PROPN
eurjchem-1090	57	11	)	)	PUNCT
eurjchem-1090	57	12	and	and	CCONJ
eurjchem-1090	57	13	moxt	moxt	NOUN
eurjchem-1090	57	14	(	(	PUNCT
eurjchem-1090	57	15	5‐200	5‐200	PROPN
eurjchem-1090	57	16	ng	ng	PROPN
eurjchem-1090	57	17	/	/	SYM
eurjchem-1090	57	18	ml	ml	PROPN
eurjchem-1090	57	19	)	)	PUNCT
eurjchem-1090	57	20	were	be	AUX
eurjchem-1090	57	21	used	use	VERB
eurjchem-1090	57	22	as	as	ADP
eurjchem-1090	57	23	the	the	DET
eurjchem-1090	57	24	calibration	calibration	NOUN
eurjchem-1090	57	25	samples	sample	NOUN
eurjchem-1090	57	26	.	.	PUNCT
eurjchem-1090	58	1	quality	quality	NOUN
eurjchem-1090	58	2	control	control	NOUN
eurjchem-1090	58	3	samples	sample	NOUN
eurjchem-1090	58	4	used	use	VERB
eurjchem-1090	58	5	were	be	AUX
eurjchem-1090	58	6	:	:	PUNCT
eurjchem-1090	58	7	0.5	0.5	NUM
eurjchem-1090	58	8	(	(	PUNCT
eurjchem-1090	58	9	lloq	lloq	PROPN
eurjchem-1090	58	10	)	)	PUNCT
eurjchem-1090	58	11	,	,	PUNCT
eurjchem-1090	58	12	15	15	NUM
eurjchem-1090	58	13	(	(	PUNCT
eurjchem-1090	58	14	lqc	lqc	PROPN
eurjchem-1090	58	15	)	)	PUNCT
eurjchem-1090	58	16	,	,	PUNCT
eurjchem-1090	58	17	50	50	NUM
eurjchem-1090	58	18	(	(	PUNCT
eurjchem-1090	58	19	mqc	mqc	NOUN
eurjchem-1090	58	20	)	)	PUNCT
eurjchem-1090	58	21	,	,	PUNCT
eurjchem-1090	58	22	100	100	NUM
eurjchem-1090	58	23	ng	ng	NOUN
eurjchem-1090	58	24	/	/	SYM
eurjchem-1090	58	25	ml	ml	PROPN
eurjchem-1090	58	26	(	(	PUNCT
eurjchem-1090	58	27	hqc	hqc	PROPN
eurjchem-1090	58	28	)	)	PUNCT
eurjchem-1090	58	29	for	for	ADP
eurjchem-1090	58	30	mox	mox	NOUN
eurjchem-1090	58	31	,	,	PUNCT
eurjchem-1090	58	32	and	and	CCONJ
eurjchem-1090	58	33	5	5	NUM
eurjchem-1090	58	34	(	(	PUNCT
eurjchem-1090	58	35	lloq	lloq	PROPN
eurjchem-1090	58	36	)	)	PUNCT
eurjchem-1090	58	37	,	,	PUNCT
eurjchem-1090	58	38	30	30	NUM
eurjchem-1090	58	39	(	(	PUNCT
eurjchem-1090	58	40	lqc	lqc	PROPN
eurjchem-1090	58	41	)	)	PUNCT
eurjchem-1090	58	42	,	,	PUNCT
eurjchem-1090	58	43	100	100	NUM
eurjchem-1090	58	44	(	(	PUNCT
eurjchem-1090	58	45	mqc	mqc	NOUN
eurjchem-1090	58	46	)	)	PUNCT
eurjchem-1090	58	47	,	,	PUNCT
eurjchem-1090	58	48	200	200	NUM
eurjchem-1090	58	49	ng	ng	NOUN
eurjchem-1090	58	50	/	/	SYM
eurjchem-1090	58	51	ml	ml	PROPN
eurjchem-1090	58	52	(	(	PUNCT
eurjchem-1090	58	53	hqc	hqc	PROPN
eurjchem-1090	58	54	)	)	PUNCT
eurjchem-1090	58	55	for	for	ADP
eurjchem-1090	58	56	moxt	moxt	NOUN
eurjchem-1090	58	57	.	.	PUNCT
eurjchem-1090	59	1	2.4	2.4	NUM
eurjchem-1090	59	2	.	.	PUNCT
eurjchem-1090	60	1	simple	simple	ADJ
eurjchem-1090	60	2	protein	protein	NOUN
eurjchem-1090	60	3	precipitation	precipitation	NOUN
eurjchem-1090	60	4	a	a	DET
eurjchem-1090	60	5	simple	simple	ADJ
eurjchem-1090	60	6	protein	protein	NOUN
eurjchem-1090	60	7	precipitation	precipitation	NOUN
eurjchem-1090	60	8	was	be	AUX
eurjchem-1090	60	9	done	do	VERB
eurjchem-1090	60	10	for	for	ADP
eurjchem-1090	60	11	extracting	extract	VERB
eurjchem-1090	60	12	mox	mox	NOUN
eurjchem-1090	60	13	,	,	PUNCT
eurjchem-1090	60	14	its	its	PRON
eurjchem-1090	60	15	active	active	ADJ
eurjchem-1090	60	16	metabolite	metabolite	NOUN
eurjchem-1090	60	17	moxt	moxt	NOUN
eurjchem-1090	60	18	,	,	PUNCT
eurjchem-1090	60	19	and	and	CCONJ
eurjchem-1090	60	20	benz	benz	PROPN
eurjchem-1090	60	21	(	(	PUNCT
eurjchem-1090	60	22	is	be	AUX
eurjchem-1090	60	23	)	)	PUNCT
eurjchem-1090	60	24	from	from	ADP
eurjchem-1090	60	25	human	human	ADJ
eurjchem-1090	60	26	plasma	plasma	NOUN
eurjchem-1090	60	27	.	.	PUNCT
eurjchem-1090	61	1	benz	benz	PROPN
eurjchem-1090	61	2	(	(	PUNCT
eurjchem-1090	61	3	is	be	AUX
eurjchem-1090	61	4	)	)	PUNCT
eurjchem-1090	61	5	solution	solution	NOUN
eurjchem-1090	61	6	(	(	PUNCT
eurjchem-1090	61	7	25	25	NUM
eurjchem-1090	61	8	µl	µl	NOUN
eurjchem-1090	61	9	of	of	ADP
eurjchem-1090	61	10	1000	1000	NUM
eurjchem-1090	61	11	ng	ng	NOUN
eurjchem-1090	61	12	/	/	SYM
eurjchem-1090	61	13	ml	ml	PROPN
eurjchem-1090	61	14	)	)	PUNCT
eurjchem-1090	61	15	was	be	AUX
eurjchem-1090	61	16	added	add	VERB
eurjchem-1090	61	17	to	to	ADP
eurjchem-1090	61	18	500	500	NUM
eurjchem-1090	61	19	µl	µl	ADP
eurjchem-1090	61	20	plasma	plasma	NOUN
eurjchem-1090	61	21	.	.	PUNCT
eurjchem-1090	62	1	acetonitrile	acetonitrile	NOUN
eurjchem-1090	62	2	(	(	PUNCT
eurjchem-1090	62	3	3	3	NUM
eurjchem-1090	62	4	ml	ml	NOUN
eurjchem-1090	62	5	)	)	PUNCT
eurjchem-1090	62	6	was	be	AUX
eurjchem-1090	62	7	added	add	VERB
eurjchem-1090	62	8	to	to	PART
eurjchem-1090	62	9	precipitate	precipitate	VERB
eurjchem-1090	62	10	plasma	plasma	NOUN
eurjchem-1090	62	11	proteins	protein	NOUN
eurjchem-1090	62	12	,	,	PUNCT
eurjchem-1090	62	13	and	and	CCONJ
eurjchem-1090	62	14	then	then	ADV
eurjchem-1090	62	15	the	the	DET
eurjchem-1090	62	16	samples	sample	NOUN
eurjchem-1090	62	17	were	be	AUX
eurjchem-1090	62	18	vortexed	vortexe	VERB
eurjchem-1090	62	19	for	for	ADP
eurjchem-1090	62	20	1	1	NUM
eurjchem-1090	62	21	min	min	NOUN
eurjchem-1090	62	22	.	.	PUNCT
eurjchem-1090	63	1	the	the	DET
eurjchem-1090	63	2	centrifugation	centrifugation	NOUN
eurjchem-1090	63	3	was	be	AUX
eurjchem-1090	63	4	done	do	VERB
eurjchem-1090	63	5	at	at	ADP
eurjchem-1090	63	6	10,000	10,000	NUM
eurjchem-1090	63	7	rpm	rpm	NOUN
eurjchem-1090	63	8	for	for	ADP
eurjchem-1090	63	9	10	10	NUM
eurjchem-1090	63	10	min	min	NOUN
eurjchem-1090	63	11	.	.	PUNCT
eurjchem-1090	64	1	the	the	DET
eurjchem-1090	64	2	clear	clear	ADJ
eurjchem-1090	64	3	supernatant	supernatant	NOUN
eurjchem-1090	64	4	was	be	AUX
eurjchem-1090	64	5	transferred	transfer	VERB
eurjchem-1090	64	6	to	to	ADP
eurjchem-1090	64	7	a	a	DET
eurjchem-1090	64	8	dry	dry	ADJ
eurjchem-1090	64	9	test	test	NOUN
eurjchem-1090	64	10	tube	tube	NOUN
eurjchem-1090	64	11	and	and	CCONJ
eurjchem-1090	64	12	evaporated	evaporate	VERB
eurjchem-1090	64	13	to	to	PART
eurjchem-1090	64	14	dryness	dryness	VERB
eurjchem-1090	64	15	under	under	ADP
eurjchem-1090	64	16	a	a	DET
eurjchem-1090	64	17	gentle	gentle	ADJ
eurjchem-1090	64	18	stream	stream	NOUN
eurjchem-1090	64	19	of	of	ADP
eurjchem-1090	64	20	nitrogen	nitrogen	NOUN
eurjchem-1090	64	21	gas	gas	NOUN
eurjchem-1090	64	22	at	at	ADP
eurjchem-1090	64	23	40	40	NUM
eurjchem-1090	64	24	°	°	NOUN
eurjchem-1090	64	25	c	c	NOUN
eurjchem-1090	64	26	,	,	PUNCT
eurjchem-1090	64	27	and	and	CCONJ
eurjchem-1090	64	28	then	then	ADV
eurjchem-1090	64	29	the	the	DET
eurjchem-1090	64	30	residue	residue	NOUN
eurjchem-1090	64	31	was	be	AUX
eurjchem-1090	64	32	reconstituted	reconstitute	VERB
eurjchem-1090	64	33	with	with	ADP
eurjchem-1090	64	34	100	100	NUM
eurjchem-1090	64	35	µl	µl	NOUN
eurjchem-1090	64	36	of	of	ADP
eurjchem-1090	64	37	the	the	DET
eurjchem-1090	64	38	mobile	mobile	ADJ
eurjchem-1090	64	39	phase	phase	NOUN
eurjchem-1090	64	40	,	,	PUNCT
eurjchem-1090	64	41	where	where	SCONJ
eurjchem-1090	64	42	only	only	ADV
eurjchem-1090	64	43	25	25	NUM
eurjchem-1090	64	44	µl	µl	NOUN
eurjchem-1090	64	45	was	be	AUX
eurjchem-1090	64	46	injected	inject	VERB
eurjchem-1090	64	47	for	for	ADP
eurjchem-1090	64	48	the	the	DET
eurjchem-1090	64	49	lc‐	lc‐	ADJ
eurjchem-1090	64	50	tandem	tandem	NOUN
eurjchem-1090	64	51	mass	mass	NOUN
eurjchem-1090	64	52	analysis	analysis	NOUN
eurjchem-1090	64	53	.	.	PUNCT
eurjchem-1090	65	1	2.5	2.5	NUM
eurjchem-1090	65	2	.	.	PUNCT
eurjchem-1090	65	3	procedures	procedure	NOUN
eurjchem-1090	65	4	2.5.1	2.5.1	NUM
eurjchem-1090	65	5	.	.	PUNCT
eurjchem-1090	66	1	stability	stability	NOUN
eurjchem-1090	66	2	of	of	ADP
eurjchem-1090	66	3	mox	mox	NOUN
eurjchem-1090	66	4	mox	mox	NOUN
eurjchem-1090	66	5	was	be	AUX
eurjchem-1090	66	6	subjected	subject	VERB
eurjchem-1090	66	7	to	to	ADP
eurjchem-1090	66	8	basic	basic	ADJ
eurjchem-1090	66	9	degradation	degradation	NOUN
eurjchem-1090	66	10	.	.	PUNCT
eurjchem-1090	67	1	standard	standard	ADJ
eurjchem-1090	67	2	mox	mox	NOUN
eurjchem-1090	67	3	powder	powder	NOUN
eurjchem-1090	67	4	(	(	PUNCT
eurjchem-1090	67	5	100	100	NUM
eurjchem-1090	67	6	mg	mg	NOUN
eurjchem-1090	67	7	)	)	PUNCT
eurjchem-1090	67	8	was	be	AUX
eurjchem-1090	67	9	weighed	weigh	VERB
eurjchem-1090	67	10	transferred	transfer	VERB
eurjchem-1090	67	11	to	to	ADP
eurjchem-1090	67	12	a	a	DET
eurjchem-1090	67	13	conical	conical	ADJ
eurjchem-1090	67	14	flask	flask	NOUN
eurjchem-1090	67	15	.	.	PUNCT
eurjchem-1090	68	1	then	then	ADV
eurjchem-1090	68	2	,	,	PUNCT
eurjchem-1090	68	3	0.1	0.1	NUM
eurjchem-1090	68	4	n	n	PRON
eurjchem-1090	68	5	naoh	naoh	NOUN
eurjchem-1090	68	6	was	be	AUX
eurjchem-1090	68	7	added	add	VERB
eurjchem-1090	68	8	on	on	ADP
eurjchem-1090	68	9	the	the	DET
eurjchem-1090	68	10	volumetric	volumetric	ADJ
eurjchem-1090	68	11	flask	flask	NOUN
eurjchem-1090	68	12	.	.	PUNCT
eurjchem-1090	69	1	then	then	ADV
eurjchem-1090	69	2	the	the	DET
eurjchem-1090	69	3	flask	flask	NOUN
eurjchem-1090	69	4	was	be	AUX
eurjchem-1090	69	5	refluxed	refluxe	VERB
eurjchem-1090	69	6	for	for	ADP
eurjchem-1090	69	7	0.5	0.5	NUM
eurjchem-1090	69	8	hour	hour	NOUN
eurjchem-1090	69	9	.	.	PUNCT
eurjchem-1090	70	1	after	after	ADP
eurjchem-1090	70	2	the	the	DET
eurjchem-1090	70	3	reflux	reflux	NOUN
eurjchem-1090	70	4	,	,	PUNCT
eurjchem-1090	70	5	the	the	DET
eurjchem-1090	70	6	conical	conical	ADJ
eurjchem-1090	70	7	flask	flask	NOUN
eurjchem-1090	70	8	was	be	AUX
eurjchem-1090	70	9	neutralized	neutralize	VERB
eurjchem-1090	70	10	against	against	ADP
eurjchem-1090	70	11	0.1	0.1	NUM
eurjchem-1090	70	12	n	n	PRON
eurjchem-1090	70	13	hcl	hcl	PROPN
eurjchem-1090	70	14	,	,	PUNCT
eurjchem-1090	70	15	then	then	ADV
eurjchem-1090	70	16	completed	complete	VERB
eurjchem-1090	70	17	to	to	ADP
eurjchem-1090	70	18	100	100	NUM
eurjchem-1090	70	19	ml	ml	NOUN
eurjchem-1090	70	20	by	by	ADP
eurjchem-1090	70	21	distilled	distilled	ADJ
eurjchem-1090	70	22	water	water	NOUN
eurjchem-1090	70	23	.	.	PUNCT
eurjchem-1090	71	1	the	the	DET
eurjchem-1090	71	2	complete	complete	ADJ
eurjchem-1090	71	3	degradation	degradation	NOUN
eurjchem-1090	71	4	was	be	AUX
eurjchem-1090	71	5	confirmed	confirm	VERB
eurjchem-1090	71	6	using	use	VERB
eurjchem-1090	71	7	hplc	hplc	NOUN
eurjchem-1090	71	8	and	and	CCONJ
eurjchem-1090	71	9	mass	mass	ADJ
eurjchem-1090	71	10	spectrometry	spectrometry	NOUN
eurjchem-1090	71	11	.	.	PUNCT
eurjchem-1090	72	1	2.5.2	2.5.2	NUM
eurjchem-1090	72	2	.	.	PUNCT
eurjchem-1090	73	1	for	for	ADP
eurjchem-1090	73	2	bulk	bulk	ADJ
eurjchem-1090	73	3	powder	powder	NOUN
eurjchem-1090	73	4	aliquot	aliquot	NOUN
eurjchem-1090	73	5	volumes	volume	NOUN
eurjchem-1090	73	6	from	from	ADP
eurjchem-1090	73	7	the	the	DET
eurjchem-1090	73	8	standard	standard	ADJ
eurjchem-1090	73	9	working	work	VERB
eurjchem-1090	73	10	solutions	solution	NOUN
eurjchem-1090	73	11	of	of	ADP
eurjchem-1090	73	12	mox	mox	NOUN
eurjchem-1090	73	13	and	and	CCONJ
eurjchem-1090	73	14	moxt	moxt	NOUN
eurjchem-1090	73	15	were	be	AUX
eurjchem-1090	73	16	accurately	accurately	ADV
eurjchem-1090	73	17	transferred	transfer	VERB
eurjchem-1090	73	18	to	to	ADP
eurjchem-1090	73	19	10	10	NUM
eurjchem-1090	73	20	ml	ml	NOUN
eurjchem-1090	73	21	volu‐	volu‐	NOUN
eurjchem-1090	73	22	metric	metric	ADJ
eurjchem-1090	73	23	flasks	flask	NOUN
eurjchem-1090	73	24	to	to	ADP
eurjchem-1090	73	25	which	which	PRON
eurjchem-1090	73	26	500	500	NUM
eurjchem-1090	73	27	µl	µl	NOUN
eurjchem-1090	73	28	of	of	ADP
eurjchem-1090	73	29	is	be	AUX
eurjchem-1090	73	30	was	be	AUX
eurjchem-1090	73	31	added	add	VERB
eurjchem-1090	73	32	to	to	PART
eurjchem-1090	73	33	provide	provide	VERB
eurjchem-1090	73	34	final	final	ADJ
eurjchem-1090	73	35	concentrations	concentration	NOUN
eurjchem-1090	73	36	of	of	ADP
eurjchem-1090	73	37	0.5‐100	0.5‐100	NUM
eurjchem-1090	73	38	ng	ng	PROPN
eurjchem-1090	73	39	/	/	SYM
eurjchem-1090	73	40	ml	ml	PROPN
eurjchem-1090	73	41	for	for	ADP
eurjchem-1090	73	42	mox	mox	NOUN
eurjchem-1090	73	43	,	,	PUNCT
eurjchem-1090	73	44	and	and	CCONJ
eurjchem-1090	73	45	5‐200	5‐200	PROPN
eurjchem-1090	73	46	ng	ng	PROPN
eurjchem-1090	73	47	/	/	SYM
eurjchem-1090	73	48	ml	ml	PROPN
eurjchem-1090	73	49	for	for	ADP
eurjchem-1090	73	50	moxt	moxt	NOUN
eurjchem-1090	73	51	.	.	PUNCT
eurjchem-1090	74	1	the	the	DET
eurjchem-1090	74	2	volume	volume	NOUN
eurjchem-1090	74	3	was	be	AUX
eurjchem-1090	74	4	completed	complete	VERB
eurjchem-1090	74	5	to	to	ADP
eurjchem-1090	74	6	the	the	DET
eurjchem-1090	74	7	volume	volume	NOUN
eurjchem-1090	74	8	by	by	ADP
eurjchem-1090	74	9	the	the	DET
eurjchem-1090	74	10	mobile	mobile	ADJ
eurjchem-1090	74	11	phase	phase	NOUN
eurjchem-1090	74	12	.	.	PUNCT
eurjchem-1090	75	1	25	25	NUM
eurjchem-1090	75	2	µl	µl	NOUN
eurjchem-1090	75	3	of	of	ADP
eurjchem-1090	75	4	each	each	DET
eurjchem-1090	75	5	concentration	concentration	NOUN
eurjchem-1090	75	6	was	be	AUX
eurjchem-1090	75	7	injected	inject	VERB
eurjchem-1090	75	8	three	three	NUM
eurjchem-1090	75	9	times	time	NOUN
eurjchem-1090	75	10	and	and	CCONJ
eurjchem-1090	75	11	following	follow	VERB
eurjchem-1090	75	12	the	the	DET
eurjchem-1090	75	13	chromatographic	chromatographic	ADJ
eurjchem-1090	75	14	conditions	condition	NOUN
eurjchem-1090	75	15	.	.	PUNCT
eurjchem-1090	76	1	2.5.3	2.5.3	X
eurjchem-1090	76	2	.	.	NOUN
eurjchem-1090	77	1	for	for	ADP
eurjchem-1090	77	2	extraction	extraction	NOUN
eurjchem-1090	77	3	from	from	ADP
eurjchem-1090	77	4	human	human	ADJ
eurjchem-1090	77	5	plasma	plasma	NOUN
eurjchem-1090	77	6	aliquot	aliquot	NOUN
eurjchem-1090	77	7	volumes	volume	NOUN
eurjchem-1090	77	8	from	from	ADP
eurjchem-1090	77	9	the	the	DET
eurjchem-1090	77	10	standard	standard	ADJ
eurjchem-1090	77	11	working	work	VERB
eurjchem-1090	77	12	solutions	solution	NOUN
eurjchem-1090	77	13	of	of	ADP
eurjchem-1090	77	14	mox	mox	NOUN
eurjchem-1090	77	15	and	and	CCONJ
eurjchem-1090	77	16	moxt	moxt	NOUN
eurjchem-1090	77	17	were	be	AUX
eurjchem-1090	77	18	added	add	VERB
eurjchem-1090	77	19	on	on	ADP
eurjchem-1090	77	20	500	500	NUM
eurjchem-1090	77	21	µl	µl	ADP
eurjchem-1090	77	22	human	human	ADJ
eurjchem-1090	77	23	plasma	plasma	NOUN
eurjchem-1090	77	24	,	,	PUNCT
eurjchem-1090	77	25	then	then	ADV
eurjchem-1090	77	26	25	25	NUM
eurjchem-1090	77	27	µl	µl	NOUN
eurjchem-1090	77	28	is	be	AUX
eurjchem-1090	77	29	was	be	AUX
eurjchem-1090	77	30	added	add	VERB
eurjchem-1090	77	31	on	on	ADP
eurjchem-1090	77	32	each	each	DET
eurjchem-1090	77	33	concentration	concentration	NOUN
eurjchem-1090	77	34	.	.	PUNCT
eurjchem-1090	78	1	then	then	ADV
eurjchem-1090	78	2	,	,	PUNCT
eurjchem-1090	78	3	3	3	NUM
eurjchem-1090	78	4	ml	ml	NOUN
eurjchem-1090	78	5	of	of	ADP
eurjchem-1090	78	6	aceto‐	aceto‐	ADJ
eurjchem-1090	78	7	nitrile	nitrile	ADV
eurjchem-1090	78	8	was	be	AUX
eurjchem-1090	78	9	added	add	VERB
eurjchem-1090	78	10	,	,	PUNCT
eurjchem-1090	78	11	the	the	DET
eurjchem-1090	78	12	samples	sample	NOUN
eurjchem-1090	78	13	were	be	AUX
eurjchem-1090	78	14	mixed	mix	VERB
eurjchem-1090	78	15	on	on	ADP
eurjchem-1090	78	16	a	a	DET
eurjchem-1090	78	17	vortex	vortex	NOUN
eurjchem-1090	78	18	for	for	ADP
eurjchem-1090	78	19	1	1	NUM
eurjchem-1090	78	20	min	min	NOUN
eurjchem-1090	78	21	,	,	PUNCT
eurjchem-1090	78	22	followed	follow	VERB
eurjchem-1090	78	23	by	by	ADP
eurjchem-1090	78	24	centrifugation	centrifugation	NOUN
eurjchem-1090	78	25	for	for	ADP
eurjchem-1090	78	26	10	10	NUM
eurjchem-1090	78	27	min	min	NOUN
eurjchem-1090	78	28	at	at	ADP
eurjchem-1090	78	29	10,000	10,000	NUM
eurjchem-1090	78	30	rpm	rpm	NOUN
eurjchem-1090	78	31	.	.	PUNCT
eurjchem-1090	79	1	the	the	DET
eurjchem-1090	79	2	clear	clear	ADJ
eurjchem-1090	79	3	supernatant	supernatant	NOUN
eurjchem-1090	79	4	was	be	AUX
eurjchem-1090	79	5	transferred	transfer	VERB
eurjchem-1090	79	6	to	to	ADP
eurjchem-1090	79	7	a	a	DET
eurjchem-1090	79	8	clean	clean	ADJ
eurjchem-1090	79	9	tube	tube	NOUN
eurjchem-1090	79	10	and	and	CCONJ
eurjchem-1090	79	11	evapora‐	evapora‐	PROPN
eurjchem-1090	79	12	ted	te	VERB
eurjchem-1090	79	13	to	to	PART
eurjchem-1090	79	14	dryness	dryness	VERB
eurjchem-1090	79	15	under	under	ADP
eurjchem-1090	79	16	a	a	DET
eurjchem-1090	79	17	gentle	gentle	ADJ
eurjchem-1090	79	18	stream	stream	NOUN
eurjchem-1090	79	19	of	of	ADP
eurjchem-1090	79	20	nitrogen	nitrogen	NOUN
eurjchem-1090	79	21	gas	gas	NOUN
eurjchem-1090	79	22	at	at	ADP
eurjchem-1090	79	23	40	40	NUM
eurjchem-1090	79	24	°	°	NOUN
eurjchem-1090	79	25	c	c	NOUN
eurjchem-1090	79	26	.	.	PUNCT
eurjchem-1090	80	1	the	the	DET
eurjchem-1090	80	2	residue	residue	NOUN
eurjchem-1090	80	3	was	be	AUX
eurjchem-1090	80	4	reconstituted	reconstitute	VERB
eurjchem-1090	80	5	with	with	ADP
eurjchem-1090	80	6	100	100	NUM
eurjchem-1090	80	7	µl	µl	ADP
eurjchem-1090	80	8	mobile	mobile	ADJ
eurjchem-1090	80	9	phase	phase	NOUN
eurjchem-1090	80	10	,	,	PUNCT
eurjchem-1090	80	11	and	and	CCONJ
eurjchem-1090	80	12	25	25	NUM
eurjchem-1090	80	13	µl	µl	NOUN
eurjchem-1090	80	14	was	be	AUX
eurjchem-1090	80	15	injected	inject	VERB
eurjchem-1090	80	16	for	for	ADP
eurjchem-1090	80	17	lc‐tandem	lc‐tandem	PROPN
eurjchem-1090	80	18	mass	mass	PROPN
eurjchem-1090	80	19	analysis	analysis	NOUN
eurjchem-1090	80	20	.	.	PUNCT
eurjchem-1090	81	1	2.6	2.6	NUM
eurjchem-1090	81	2	.	.	PUNCT
eurjchem-1090	81	3	method	method	NOUN
eurjchem-1090	81	4	validation	validation	NOUN
eurjchem-1090	81	5	the	the	DET
eurjchem-1090	81	6	validation	validation	NOUN
eurjchem-1090	81	7	of	of	ADP
eurjchem-1090	81	8	the	the	DET
eurjchem-1090	81	9	proposed	propose	VERB
eurjchem-1090	81	10	method	method	NOUN
eurjchem-1090	81	11	was	be	AUX
eurjchem-1090	81	12	done	do	VERB
eurjchem-1090	81	13	as	as	ADP
eurjchem-1090	81	14	per	per	ADP
eurjchem-1090	81	15	the	the	DET
eurjchem-1090	81	16	fda	fda	PROPN
eurjchem-1090	81	17	guidelines	guideline	NOUN
eurjchem-1090	81	18	.	.	PUNCT
eurjchem-1090	82	1	2.6.1	2.6.1	X
eurjchem-1090	82	2	.	.	PUNCT
eurjchem-1090	83	1	selectivity	selectivity	NOUN
eurjchem-1090	83	2	blank	blank	ADP
eurjchem-1090	83	3	human	human	ADJ
eurjchem-1090	83	4	plasma	plasma	NOUN
eurjchem-1090	83	5	from	from	ADP
eurjchem-1090	83	6	six	six	NUM
eurjchem-1090	83	7	different	different	ADJ
eurjchem-1090	83	8	sources	source	NOUN
eurjchem-1090	83	9	were	be	AUX
eurjchem-1090	83	10	tested	test	VERB
eurjchem-1090	83	11	for	for	ADP
eurjchem-1090	83	12	any	any	DET
eurjchem-1090	83	13	interference	interference	NOUN
eurjchem-1090	83	14	of	of	ADP
eurjchem-1090	83	15	endogenous	endogenous	ADJ
eurjchem-1090	83	16	plasma	plasma	NOUN
eurjchem-1090	83	17	constituents	constituent	NOUN
eurjchem-1090	83	18	with	with	ADP
eurjchem-1090	83	19	the	the	DET
eurjchem-1090	83	20	analytes	analyte	NOUN
eurjchem-1090	83	21	and	and	CCONJ
eurjchem-1090	83	22	the	the	PRON
eurjchem-1090	83	23	is	be	AUX
eurjchem-1090	83	24	.	.	PUNCT
eurjchem-1090	84	1	664	664	NUM
eurjchem-1090	84	2	elaziz	elaziz	NOUN
eurjchem-1090	84	3	et	et	PROPN
eurjchem-1090	84	4	al	al	PROPN
eurjchem-1090	84	5	.	.	PUNCT
eurjchem-1090	84	6	/	/	SYM
eurjchem-1090	84	7	european	european	PROPN
eurjchem-1090	84	8	journal	journal	PROPN
eurjchem-1090	84	9	of	of	ADP
eurjchem-1090	84	10	chemistry	chemistry	NOUN
eurjchem-1090	84	11	5	5	NUM
eurjchem-1090	84	12	(	(	PUNCT
eurjchem-1090	84	13	4	4	NUM
eurjchem-1090	84	14	)	)	PUNCT
eurjchem-1090	84	15	(	(	PUNCT
eurjchem-1090	84	16	2014	2014	NUM
eurjchem-1090	84	17	)	)	PUNCT
eurjchem-1090	84	18	662‐667	662‐667	PROPN
eurjchem-1090	84	19	2.6.2	2.6.2	NUM
eurjchem-1090	84	20	.	.	PUNCT
eurjchem-1090	84	21	matrix	matrix	NOUN
eurjchem-1090	84	22	effect	effect	NOUN
eurjchem-1090	84	23	it	it	PRON
eurjchem-1090	84	24	is	be	AUX
eurjchem-1090	84	25	the	the	DET
eurjchem-1090	84	26	effect	effect	NOUN
eurjchem-1090	84	27	of	of	ADP
eurjchem-1090	84	28	the	the	DET
eurjchem-1090	84	29	matrix	matrix	NOUN
eurjchem-1090	84	30	which	which	PRON
eurjchem-1090	84	31	contains	contain	VERB
eurjchem-1090	84	32	the	the	DET
eurjchem-1090	84	33	analysed	analyse	VERB
eurjchem-1090	84	34	sample	sample	NOUN
eurjchem-1090	84	35	on	on	ADP
eurjchem-1090	84	36	the	the	DET
eurjchem-1090	84	37	sample	sample	NOUN
eurjchem-1090	84	38	determination	determination	NOUN
eurjchem-1090	84	39	.	.	PUNCT
eurjchem-1090	85	1	to	to	PART
eurjchem-1090	85	2	test	test	VERB
eurjchem-1090	85	3	for	for	ADP
eurjchem-1090	85	4	the	the	DET
eurjchem-1090	85	5	effect	effect	NOUN
eurjchem-1090	85	6	of	of	ADP
eurjchem-1090	85	7	the	the	DET
eurjchem-1090	85	8	studied	study	VERB
eurjchem-1090	85	9	matrix	matrix	NOUN
eurjchem-1090	85	10	on	on	ADP
eurjchem-1090	85	11	the	the	DET
eurjchem-1090	85	12	quantitative	quantitative	ADJ
eurjchem-1090	85	13	determination	determination	NOUN
eurjchem-1090	85	14	of	of	ADP
eurjchem-1090	85	15	the	the	DET
eurjchem-1090	85	16	analytes	analyte	NOUN
eurjchem-1090	85	17	,	,	PUNCT
eurjchem-1090	85	18	extraction	extraction	NOUN
eurjchem-1090	85	19	was	be	AUX
eurjchem-1090	85	20	done	do	VERB
eurjchem-1090	85	21	to	to	PART
eurjchem-1090	85	22	blank	blank	VERB
eurjchem-1090	85	23	human	human	ADJ
eurjchem-1090	85	24	plasma	plasma	NOUN
eurjchem-1090	85	25	samples	sample	NOUN
eurjchem-1090	85	26	as	as	SCONJ
eurjchem-1090	85	27	explained	explain	VERB
eurjchem-1090	85	28	earlier	early	ADV
eurjchem-1090	85	29	,	,	PUNCT
eurjchem-1090	85	30	and	and	CCONJ
eurjchem-1090	85	31	after	after	ADP
eurjchem-1090	85	32	the	the	DET
eurjchem-1090	85	33	extraction	extraction	NOUN
eurjchem-1090	85	34	step	step	NOUN
eurjchem-1090	85	35	,	,	PUNCT
eurjchem-1090	85	36	the	the	DET
eurjchem-1090	85	37	samples	sample	NOUN
eurjchem-1090	85	38	were	be	AUX
eurjchem-1090	85	39	spiked	spike	VERB
eurjchem-1090	85	40	with	with	ADP
eurjchem-1090	85	41	three	three	NUM
eurjchem-1090	85	42	different	different	ADJ
eurjchem-1090	85	43	quality	quality	NOUN
eurjchem-1090	85	44	control	control	NOUN
eurjchem-1090	85	45	levels	level	NOUN
eurjchem-1090	85	46	with	with	ADP
eurjchem-1090	85	47	the	the	PRON
eurjchem-1090	85	48	is	be	AUX
eurjchem-1090	85	49	in	in	ADP
eurjchem-1090	85	50	triplicates	triplicate	NOUN
eurjchem-1090	85	51	.	.	PUNCT
eurjchem-1090	86	1	then	then	ADV
eurjchem-1090	86	2	the	the	DET
eurjchem-1090	86	3	samples	sample	NOUN
eurjchem-1090	86	4	were	be	AUX
eurjchem-1090	86	5	sent	send	VERB
eurjchem-1090	86	6	for	for	ADP
eurjchem-1090	86	7	analysis	analysis	NOUN
eurjchem-1090	86	8	to	to	PART
eurjchem-1090	86	9	obtain	obtain	VERB
eurjchem-1090	86	10	the	the	DET
eurjchem-1090	86	11	peak	peak	NOUN
eurjchem-1090	86	12	areas	area	NOUN
eurjchem-1090	86	13	.	.	PUNCT
eurjchem-1090	87	1	the	the	DET
eurjchem-1090	87	2	peak	peak	NOUN
eurjchem-1090	87	3	areas	area	NOUN
eurjchem-1090	87	4	obtained	obtain	VERB
eurjchem-1090	87	5	were	be	AUX
eurjchem-1090	87	6	compared	compare	VERB
eurjchem-1090	87	7	with	with	ADP
eurjchem-1090	87	8	those	those	PRON
eurjchem-1090	87	9	obtained	obtain	VERB
eurjchem-1090	87	10	from	from	ADP
eurjchem-1090	87	11	standard	standard	ADJ
eurjchem-1090	87	12	solutions	solution	NOUN
eurjchem-1090	87	13	,	,	PUNCT
eurjchem-1090	87	14	where	where	SCONJ
eurjchem-1090	87	15	matrix	matrix	NOUN
eurjchem-1090	87	16	effect	effect	NOUN
eurjchem-1090	87	17	is	be	AUX
eurjchem-1090	87	18	the	the	DET
eurjchem-1090	87	19	peak	peak	NOUN
eurjchem-1090	87	20	area	area	NOUN
eurjchem-1090	87	21	ratio	ratio	NOUN
eurjchem-1090	87	22	.	.	PUNCT
eurjchem-1090	88	1	matrix	matrix	NOUN
eurjchem-1090	88	2	effect	effect	NOUN
eurjchem-1090	88	3	is	be	AUX
eurjchem-1090	88	4	usually	usually	ADV
eurjchem-1090	88	5	done	do	VERB
eurjchem-1090	88	6	to	to	PART
eurjchem-1090	88	7	ensure	ensure	VERB
eurjchem-1090	88	8	the	the	DET
eurjchem-1090	88	9	precision	precision	NOUN
eurjchem-1090	88	10	and	and	CCONJ
eurjchem-1090	88	11	repeatability	repeatability	NOUN
eurjchem-1090	88	12	of	of	ADP
eurjchem-1090	88	13	the	the	DET
eurjchem-1090	88	14	method	method	NOUN
eurjchem-1090	88	15	.	.	PUNCT
eurjchem-1090	89	1	2.6.3	2.6.3	NUM
eurjchem-1090	89	2	.	.	PUNCT
eurjchem-1090	89	3	recovery	recovery	NOUN
eurjchem-1090	89	4	calculation	calculation	NOUN
eurjchem-1090	89	5	of	of	ADP
eurjchem-1090	89	6	the	the	DET
eurjchem-1090	89	7	recovery	recovery	NOUN
eurjchem-1090	89	8	%	%	NOUN
eurjchem-1090	89	9	is	be	AUX
eurjchem-1090	89	10	done	do	VERB
eurjchem-1090	89	11	to	to	PART
eurjchem-1090	89	12	test	test	VERB
eurjchem-1090	89	13	for	for	ADP
eurjchem-1090	89	14	the	the	DET
eurjchem-1090	89	15	extraction	extraction	NOUN
eurjchem-1090	89	16	efficiency	efficiency	NOUN
eurjchem-1090	89	17	of	of	ADP
eurjchem-1090	89	18	the	the	DET
eurjchem-1090	89	19	method	method	NOUN
eurjchem-1090	89	20	.	.	PUNCT
eurjchem-1090	90	1	the	the	DET
eurjchem-1090	90	2	extraction	extraction	NOUN
eurjchem-1090	90	3	procedure	procedure	NOUN
eurjchem-1090	90	4	was	be	AUX
eurjchem-1090	90	5	done	do	VERB
eurjchem-1090	90	6	as	as	SCONJ
eurjchem-1090	90	7	mentioned	mention	VERB
eurjchem-1090	90	8	above	above	ADV
eurjchem-1090	90	9	for	for	ADP
eurjchem-1090	90	10	the	the	DET
eurjchem-1090	90	11	spiked	spiked	ADJ
eurjchem-1090	90	12	plasma	plasma	NOUN
eurjchem-1090	90	13	samples	sample	NOUN
eurjchem-1090	90	14	and	and	CCONJ
eurjchem-1090	90	15	the	the	DET
eurjchem-1090	90	16	peak	peak	NOUN
eurjchem-1090	90	17	areas	area	NOUN
eurjchem-1090	90	18	were	be	AUX
eurjchem-1090	90	19	calculated	calculate	VERB
eurjchem-1090	90	20	.	.	PUNCT
eurjchem-1090	91	1	then	then	ADV
eurjchem-1090	91	2	the	the	DET
eurjchem-1090	91	3	peak	peak	NOUN
eurjchem-1090	91	4	areas	area	NOUN
eurjchem-1090	91	5	of	of	ADP
eurjchem-1090	91	6	samples	sample	NOUN
eurjchem-1090	91	7	spiked	spike	VERB
eurjchem-1090	91	8	after	after	SCONJ
eurjchem-1090	91	9	the	the	DET
eurjchem-1090	91	10	extraction	extraction	NOUN
eurjchem-1090	91	11	step	step	NOUN
eurjchem-1090	91	12	was	be	AUX
eurjchem-1090	91	13	calculated	calculate	VERB
eurjchem-1090	91	14	.	.	PUNCT
eurjchem-1090	92	1	the	the	DET
eurjchem-1090	92	2	ratio	ratio	NOUN
eurjchem-1090	92	3	of	of	ADP
eurjchem-1090	92	4	the	the	DET
eurjchem-1090	92	5	two	two	NUM
eurjchem-1090	92	6	peaks	peak	NOUN
eurjchem-1090	92	7	was	be	AUX
eurjchem-1090	92	8	the	the	DET
eurjchem-1090	92	9	recovery	recovery	NOUN
eurjchem-1090	92	10	%	%	NOUN
eurjchem-1090	92	11	.	.	PUNCT
eurjchem-1090	93	1	this	this	PRON
eurjchem-1090	93	2	was	be	AUX
eurjchem-1090	93	3	done	do	VERB
eurjchem-1090	93	4	at	at	ADP
eurjchem-1090	93	5	three	three	NUM
eurjchem-1090	93	6	quality	quality	NOUN
eurjchem-1090	93	7	control	control	NOUN
eurjchem-1090	93	8	levels	level	NOUN
eurjchem-1090	93	9	in	in	ADP
eurjchem-1090	93	10	triplicates	triplicate	NOUN
eurjchem-1090	93	11	.	.	PUNCT
eurjchem-1090	94	1	2.6.4	2.6.4	NUM
eurjchem-1090	94	2	.	.	PUNCT
eurjchem-1090	95	1	calibration	calibration	NOUN
eurjchem-1090	95	2	curves	curve	NOUN
eurjchem-1090	95	3	samples	sample	NOUN
eurjchem-1090	95	4	used	use	VERB
eurjchem-1090	95	5	for	for	ADP
eurjchem-1090	95	6	calibration	calibration	NOUN
eurjchem-1090	95	7	consist	consist	NOUN
eurjchem-1090	95	8	of	of	ADP
eurjchem-1090	95	9	six	six	NUM
eurjchem-1090	95	10	concentrations	concentration	NOUN
eurjchem-1090	95	11	of	of	ADP
eurjchem-1090	95	12	mox	mox	NOUN
eurjchem-1090	95	13	(	(	PUNCT
eurjchem-1090	95	14	0.5‐100	0.5‐100	NUM
eurjchem-1090	95	15	ng	ng	PROPN
eurjchem-1090	95	16	/	/	SYM
eurjchem-1090	95	17	ml	ml	PROPN
eurjchem-1090	95	18	)	)	PUNCT
eurjchem-1090	95	19	and	and	CCONJ
eurjchem-1090	95	20	moxt	moxt	NOUN
eurjchem-1090	95	21	(	(	PUNCT
eurjchem-1090	95	22	5‐200	5‐200	PROPN
eurjchem-1090	95	23	ng	ng	PROPN
eurjchem-1090	95	24	/	/	SYM
eurjchem-1090	95	25	ml	ml	PROPN
eurjchem-1090	95	26	)	)	PUNCT
eurjchem-1090	95	27	.	.	PUNCT
eurjchem-1090	96	1	each	each	DET
eurjchem-1090	96	2	concentration	concentration	NOUN
eurjchem-1090	96	3	was	be	AUX
eurjchem-1090	96	4	injected	inject	VERB
eurjchem-1090	96	5	three	three	NUM
eurjchem-1090	96	6	times	time	NOUN
eurjchem-1090	96	7	.	.	PUNCT
eurjchem-1090	97	1	the	the	DET
eurjchem-1090	97	2	relative	relative	ADJ
eurjchem-1090	97	3	peak	peak	PROPN
eurjchem-1090	97	4	area	area	NOUN
eurjchem-1090	97	5	of	of	ADP
eurjchem-1090	97	6	each	each	DET
eurjchem-1090	97	7	analyte	analyte	NOUN
eurjchem-1090	97	8	was	be	AUX
eurjchem-1090	97	9	recorded	record	VERB
eurjchem-1090	97	10	against	against	ADP
eurjchem-1090	97	11	its	its	PRON
eurjchem-1090	97	12	concentration	concentration	NOUN
eurjchem-1090	97	13	,	,	PUNCT
eurjchem-1090	97	14	the	the	DET
eurjchem-1090	97	15	linearity	linearity	NOUN
eurjchem-1090	97	16	curves	curve	NOUN
eurjchem-1090	97	17	were	be	AUX
eurjchem-1090	97	18	constructed	construct	VERB
eurjchem-1090	97	19	and	and	CCONJ
eurjchem-1090	97	20	the	the	DET
eurjchem-1090	97	21	regression	regression	NOUN
eurjchem-1090	97	22	equations	equation	NOUN
eurjchem-1090	97	23	computed	compute	VERB
eurjchem-1090	97	24	.	.	PUNCT
eurjchem-1090	98	1	2.6.5	2.6.5	X
eurjchem-1090	98	2	.	.	X
eurjchem-1090	98	3	precision	precision	NOUN
eurjchem-1090	98	4	and	and	CCONJ
eurjchem-1090	98	5	accuracy	accuracy	NOUN
eurjchem-1090	98	6	three	three	NUM
eurjchem-1090	98	7	different	different	ADJ
eurjchem-1090	98	8	qc	qc	PROPN
eurjchem-1090	98	9	levels	level	NOUN
eurjchem-1090	98	10	of	of	ADP
eurjchem-1090	98	11	each	each	DET
eurjchem-1090	98	12	analyte	analyte	NOUN
eurjchem-1090	98	13	were	be	AUX
eurjchem-1090	98	14	analysed	analyse	VERB
eurjchem-1090	98	15	three	three	NUM
eurjchem-1090	98	16	times	time	NOUN
eurjchem-1090	98	17	intra‐daily	intra‐daily	ADV
eurjchem-1090	98	18	using	use	VERB
eurjchem-1090	98	19	the	the	DET
eurjchem-1090	98	20	proposed	propose	VERB
eurjchem-1090	98	21	methods	method	NOUN
eurjchem-1090	98	22	under	under	ADP
eurjchem-1090	98	23	the	the	DET
eurjchem-1090	98	24	same	same	ADJ
eurjchem-1090	98	25	experimental	experimental	ADJ
eurjchem-1090	98	26	conditions	condition	NOUN
eurjchem-1090	98	27	to	to	PART
eurjchem-1090	98	28	estimate	estimate	VERB
eurjchem-1090	98	29	precision	precision	NOUN
eurjchem-1090	98	30	and	and	CCONJ
eurjchem-1090	98	31	accuracy	accuracy	NOUN
eurjchem-1090	98	32	.	.	PUNCT
eurjchem-1090	99	1	the	the	DET
eurjchem-1090	99	2	previous	previous	ADJ
eurjchem-1090	99	3	procedures	procedure	NOUN
eurjchem-1090	99	4	were	be	AUX
eurjchem-1090	99	5	repeated	repeat	VERB
eurjchem-1090	99	6	inter‐daily	inter‐daily	ADV
eurjchem-1090	99	7	on	on	ADP
eurjchem-1090	99	8	three	three	NUM
eurjchem-1090	99	9	different	different	ADJ
eurjchem-1090	99	10	days	day	NOUN
eurjchem-1090	99	11	for	for	ADP
eurjchem-1090	99	12	the	the	DET
eurjchem-1090	99	13	analysis	analysis	NOUN
eurjchem-1090	99	14	of	of	ADP
eurjchem-1090	99	15	the	the	DET
eurjchem-1090	99	16	three	three	NUM
eurjchem-1090	99	17	chosen	choose	VERB
eurjchem-1090	99	18	concentrations	concentration	NOUN
eurjchem-1090	99	19	to	to	PART
eurjchem-1090	99	20	calculate	calculate	VERB
eurjchem-1090	99	21	the	the	DET
eurjchem-1090	99	22	inter‐assay	inter‐assay	PROPN
eurjchem-1090	99	23	precision	precision	NOUN
eurjchem-1090	99	24	.	.	PUNCT
eurjchem-1090	100	1	the	the	DET
eurjchem-1090	100	2	relative	relative	ADJ
eurjchem-1090	100	3	standard	standard	ADJ
eurjchem-1090	100	4	deviations	deviation	NOUN
eurjchem-1090	100	5	were	be	AUX
eurjchem-1090	100	6	calculated	calculate	VERB
eurjchem-1090	100	7	.	.	PUNCT
eurjchem-1090	101	1	the	the	DET
eurjchem-1090	101	2	criteria	criterion	NOUN
eurjchem-1090	101	3	for	for	ADP
eurjchem-1090	101	4	acceptability	acceptability	NOUN
eurjchem-1090	101	5	of	of	ADP
eurjchem-1090	101	6	data	datum	NOUN
eurjchem-1090	101	7	were	be	AUX
eurjchem-1090	101	8	accuracy	accuracy	NOUN
eurjchem-1090	101	9	within	within	ADP
eurjchem-1090	101	10	±15	±15	NOUN
eurjchem-1090	101	11	%	%	NOUN
eurjchem-1090	101	12	from	from	ADP
eurjchem-1090	101	13	the	the	DET
eurjchem-1090	101	14	nominal	nominal	ADJ
eurjchem-1090	101	15	values	value	NOUN
eurjchem-1090	101	16	and	and	CCONJ
eurjchem-1090	101	17	a	a	DET
eurjchem-1090	101	18	precision	precision	NOUN
eurjchem-1090	101	19	of	of	ADP
eurjchem-1090	101	20	within	within	ADP
eurjchem-1090	101	21	±15	±15	NOUN
eurjchem-1090	101	22	%	%	NOUN
eurjchem-1090	101	23	relative	relative	ADJ
eurjchem-1090	101	24	standard	standard	ADJ
eurjchem-1090	101	25	deviation	deviation	NOUN
eurjchem-1090	101	26	(	(	PUNCT
eurjchem-1090	101	27	rsd	rsd	NOUN
eurjchem-1090	101	28	)	)	PUNCT
eurjchem-1090	101	29	,	,	PUNCT
eurjchem-1090	101	30	but	but	CCONJ
eurjchem-1090	101	31	that	that	PRON
eurjchem-1090	101	32	of	of	ADP
eurjchem-1090	101	33	lqc	lqc	NOUN
eurjchem-1090	101	34	is	be	AUX
eurjchem-1090	101	35	not	not	PART
eurjchem-1090	101	36	supposed	suppose	VERB
eurjchem-1090	101	37	to	to	PART
eurjchem-1090	101	38	exceed	exceed	VERB
eurjchem-1090	101	39	±20	±20	PROPN
eurjchem-1090	101	40	%	%	NOUN
eurjchem-1090	101	41	(	(	PUNCT
eurjchem-1090	101	42	us	us	PROPN
eurjchem-1090	101	43	dhhs	dhhs	PROPN
eurjchem-1090	101	44	,	,	PUNCT
eurjchem-1090	101	45	fda	fda	PROPN
eurjchem-1090	101	46	,	,	PUNCT
eurjchem-1090	101	47	cder	cder	NOUN
eurjchem-1090	101	48	,	,	PUNCT
eurjchem-1090	101	49	2001	2001	NUM
eurjchem-1090	101	50	)	)	PUNCT
eurjchem-1090	102	1	[	[	X
eurjchem-1090	102	2	12	12	NUM
eurjchem-1090	102	3	]	]	PUNCT
eurjchem-1090	102	4	.	.	PUNCT
eurjchem-1090	103	1	2.6.6	2.6.6	NUM
eurjchem-1090	103	2	.	.	PUNCT
eurjchem-1090	104	1	stability	stability	PROPN
eurjchem-1090	104	2	2.6.6.1	2.6.6.1	NUM
eurjchem-1090	104	3	.	.	PUNCT
eurjchem-1090	105	1	short‐term	short‐term	ADJ
eurjchem-1090	105	2	stability	stability	NOUN
eurjchem-1090	105	3	to	to	PART
eurjchem-1090	105	4	test	test	VERB
eurjchem-1090	105	5	for	for	ADP
eurjchem-1090	105	6	the	the	DET
eurjchem-1090	105	7	short	short	ADJ
eurjchem-1090	105	8	term	term	NOUN
eurjchem-1090	105	9	stability	stability	NOUN
eurjchem-1090	105	10	of	of	ADP
eurjchem-1090	105	11	the	the	DET
eurjchem-1090	105	12	analytes	analyte	NOUN
eurjchem-1090	105	13	,	,	PUNCT
eurjchem-1090	105	14	three	three	NUM
eurjchem-1090	105	15	quality	quality	NOUN
eurjchem-1090	105	16	control	control	NOUN
eurjchem-1090	105	17	levels	level	NOUN
eurjchem-1090	105	18	were	be	AUX
eurjchem-1090	105	19	left	leave	VERB
eurjchem-1090	105	20	for	for	ADP
eurjchem-1090	105	21	8	8	NUM
eurjchem-1090	105	22	hours	hour	NOUN
eurjchem-1090	105	23	on	on	ADP
eurjchem-1090	105	24	bench	bench	NOUN
eurjchem-1090	105	25	top	top	NOUN
eurjchem-1090	105	26	at	at	ADP
eurjchem-1090	105	27	room	room	NOUN
eurjchem-1090	105	28	temperature	temperature	NOUN
eurjchem-1090	105	29	(	(	PUNCT
eurjchem-1090	105	30	bench‐top	bench‐top	NOUN
eurjchem-1090	105	31	stability	stability	NOUN
eurjchem-1090	105	32	)	)	PUNCT
eurjchem-1090	105	33	.	.	PUNCT
eurjchem-1090	106	1	this	this	PRON
eurjchem-1090	106	2	was	be	AUX
eurjchem-1090	106	3	done	do	VERB
eurjchem-1090	106	4	in	in	ADP
eurjchem-1090	106	5	triplicates	triplicate	NOUN
eurjchem-1090	106	6	.	.	PUNCT
eurjchem-1090	107	1	2.6.6.2	2.6.6.2	NUM
eurjchem-1090	107	2	.	.	PUNCT
eurjchem-1090	108	1	freeze	freeze	NOUN
eurjchem-1090	108	2	and	and	CCONJ
eurjchem-1090	108	3	thaw	thaw	NOUN
eurjchem-1090	108	4	stability	stability	NOUN
eurjchem-1090	108	5	three	three	NUM
eurjchem-1090	108	6	freeze	freeze	NOUN
eurjchem-1090	108	7	and	and	CCONJ
eurjchem-1090	108	8	thaw	thaw	NOUN
eurjchem-1090	108	9	cycles	cycle	NOUN
eurjchem-1090	108	10	were	be	AUX
eurjchem-1090	108	11	applied	apply	VERB
eurjchem-1090	108	12	to	to	PART
eurjchem-1090	108	13	test	test	VERB
eurjchem-1090	108	14	for	for	ADP
eurjchem-1090	108	15	the	the	DET
eurjchem-1090	108	16	analytes	analyte	NOUN
eurjchem-1090	108	17	’	'	PUNCT
eurjchem-1090	108	18	stability	stability	NOUN
eurjchem-1090	108	19	.	.	PUNCT
eurjchem-1090	109	1	the	the	DET
eurjchem-1090	109	2	general	general	ADJ
eurjchem-1090	109	3	procedure	procedure	NOUN
eurjchem-1090	109	4	mentioned	mention	VERB
eurjchem-1090	109	5	above	above	ADV
eurjchem-1090	109	6	was	be	AUX
eurjchem-1090	109	7	applied	apply	VERB
eurjchem-1090	109	8	for	for	ADP
eurjchem-1090	109	9	the	the	DET
eurjchem-1090	109	10	analysis	analysis	NOUN
eurjchem-1090	109	11	.	.	PUNCT
eurjchem-1090	110	1	the	the	DET
eurjchem-1090	110	2	same	same	ADJ
eurjchem-1090	110	3	criteria	criterion	NOUN
eurjchem-1090	110	4	of	of	ADP
eurjchem-1090	110	5	data	datum	NOUN
eurjchem-1090	110	6	acceptance	acceptance	NOUN
eurjchem-1090	110	7	mentioned	mention	VERB
eurjchem-1090	110	8	under	under	ADP
eurjchem-1090	110	9	precision	precision	NOUN
eurjchem-1090	110	10	apply	apply	VERB
eurjchem-1090	110	11	here	here	ADV
eurjchem-1090	110	12	.	.	PUNCT
eurjchem-1090	111	1	2.6.6.3	2.6.6.3	X
eurjchem-1090	111	2	.	.	PUNCT
eurjchem-1090	111	3	stock	stock	NOUN
eurjchem-1090	111	4	solution	solution	NOUN
eurjchem-1090	111	5	stability	stability	NOUN
eurjchem-1090	111	6	the	the	DET
eurjchem-1090	111	7	stability	stability	NOUN
eurjchem-1090	111	8	of	of	ADP
eurjchem-1090	111	9	mox	mox	PROPN
eurjchem-1090	111	10	,	,	PUNCT
eurjchem-1090	111	11	moxt	moxt	NOUN
eurjchem-1090	111	12	,	,	PUNCT
eurjchem-1090	111	13	and	and	CCONJ
eurjchem-1090	111	14	i.s	i.s	PROPN
eurjchem-1090	111	15	stock	stock	NOUN
eurjchem-1090	111	16	solutions	solution	NOUN
eurjchem-1090	111	17	was	be	AUX
eurjchem-1090	111	18	performed	perform	VERB
eurjchem-1090	111	19	by	by	ADP
eurjchem-1090	111	20	comparison	comparison	NOUN
eurjchem-1090	111	21	of	of	ADP
eurjchem-1090	111	22	results	result	NOUN
eurjchem-1090	111	23	from	from	ADP
eurjchem-1090	111	24	a	a	DET
eurjchem-1090	111	25	solution	solution	NOUN
eurjchem-1090	111	26	kept	keep	VERB
eurjchem-1090	111	27	for	for	ADP
eurjchem-1090	111	28	about	about	ADV
eurjchem-1090	111	29	60	60	NUM
eurjchem-1090	111	30	days	day	NOUN
eurjchem-1090	111	31	at	at	ADP
eurjchem-1090	111	32	4	4	NUM
eurjchem-1090	111	33	°	°	NOUN
eurjchem-1090	111	34	c	c	NOUN
eurjchem-1090	111	35	and	and	CCONJ
eurjchem-1090	111	36	from	from	ADP
eurjchem-1090	111	37	a	a	DET
eurjchem-1090	111	38	solution	solution	NOUN
eurjchem-1090	111	39	that	that	PRON
eurjchem-1090	111	40	was	be	AUX
eurjchem-1090	111	41	extem‐	extem‐	X
eurjchem-1090	111	42	poraneously	poraneously	ADV
eurjchem-1090	111	43	prepared	prepare	VERB
eurjchem-1090	111	44	.	.	PUNCT
eurjchem-1090	112	1	for	for	ADP
eurjchem-1090	112	2	this	this	DET
eurjchem-1090	112	3	purpose	purpose	NOUN
eurjchem-1090	112	4	,	,	PUNCT
eurjchem-1090	112	5	three	three	NUM
eurjchem-1090	112	6	replicates	replicate	NOUN
eurjchem-1090	112	7	of	of	ADP
eurjchem-1090	112	8	each	each	DET
eurjchem-1090	112	9	analyte	analyte	NOUN
eurjchem-1090	112	10	were	be	AUX
eurjchem-1090	112	11	prepared	prepare	VERB
eurjchem-1090	112	12	from	from	ADP
eurjchem-1090	112	13	each	each	DET
eurjchem-1090	112	14	stock	stock	NOUN
eurjchem-1090	112	15	solution	solution	NOUN
eurjchem-1090	112	16	and	and	CCONJ
eurjchem-1090	112	17	injected	inject	VERB
eurjchem-1090	112	18	in	in	ADP
eurjchem-1090	112	19	the	the	DET
eurjchem-1090	112	20	lc‐ms	lc‐ms	NOUN
eurjchem-1090	112	21	/	/	SYM
eurjchem-1090	112	22	ms	ms	NOUN
eurjchem-1090	112	23	system	system	NOUN
eurjchem-1090	112	24	.	.	PUNCT
eurjchem-1090	113	1	the	the	DET
eurjchem-1090	113	2	same	same	ADJ
eurjchem-1090	113	3	test	test	NOUN
eurjchem-1090	113	4	was	be	AUX
eurjchem-1090	113	5	performed	perform	VERB
eurjchem-1090	113	6	with	with	ADP
eurjchem-1090	113	7	the	the	DET
eurjchem-1090	113	8	stock	stock	NOUN
eurjchem-1090	113	9	solutions	solution	NOUN
eurjchem-1090	113	10	of	of	ADP
eurjchem-1090	113	11	i.s	i.s	PROPN
eurjchem-1090	113	12	.	.	PROPN
eurjchem-1090	113	13	results	result	NOUN
eurjchem-1090	113	14	were	be	AUX
eurjchem-1090	113	15	compared	compare	VERB
eurjchem-1090	113	16	to	to	ADP
eurjchem-1090	113	17	freshly	freshly	ADV
eurjchem-1090	113	18	prepared	prepare	VERB
eurjchem-1090	113	19	solutions	solution	NOUN
eurjchem-1090	113	20	at	at	ADP
eurjchem-1090	113	21	corresponding	corresponding	ADJ
eurjchem-1090	113	22	concentration	concentration	NOUN
eurjchem-1090	113	23	.	.	PUNCT
eurjchem-1090	114	1	the	the	DET
eurjchem-1090	114	2	samples	sample	NOUN
eurjchem-1090	114	3	qualified	qualify	VERB
eurjchem-1090	114	4	the	the	DET
eurjchem-1090	114	5	test	test	NOUN
eurjchem-1090	114	6	if	if	SCONJ
eurjchem-1090	114	7	the	the	DET
eurjchem-1090	114	8	deviation	deviation	NOUN
eurjchem-1090	114	9	was	be	AUX
eurjchem-1090	114	10	within	within	ADP
eurjchem-1090	114	11	±15	±15	NOUN
eurjchem-1090	114	12	%	%	NOUN
eurjchem-1090	114	13	.	.	PUNCT
eurjchem-1090	115	1	3	3	X
eurjchem-1090	115	2	.	.	NOUN
eurjchem-1090	115	3	results	result	NOUN
eurjchem-1090	115	4	and	and	CCONJ
eurjchem-1090	115	5	discussion	discussion	NOUN
eurjchem-1090	115	6	3.1	3.1	NUM
eurjchem-1090	115	7	.	.	PUNCT
eurjchem-1090	116	1	method	method	NOUN
eurjchem-1090	116	2	development	development	NOUN
eurjchem-1090	116	3	3.1.1	3.1.1	NUM
eurjchem-1090	116	4	.	.	PUNCT
eurjchem-1090	117	1	mass	mass	ADJ
eurjchem-1090	117	2	spectrometry	spectrometry	NOUN
eurjchem-1090	117	3	both	both	CCONJ
eurjchem-1090	117	4	positive	positive	ADJ
eurjchem-1090	117	5	and	and	CCONJ
eurjchem-1090	117	6	negative	negative	ADJ
eurjchem-1090	117	7	ion	ion	NOUN
eurjchem-1090	117	8	modes	mode	NOUN
eurjchem-1090	117	9	were	be	AUX
eurjchem-1090	117	10	tried	try	VERB
eurjchem-1090	117	11	for	for	ADP
eurjchem-1090	117	12	the	the	DET
eurjchem-1090	117	13	simultaneous	simultaneous	ADJ
eurjchem-1090	117	14	determination	determination	NOUN
eurjchem-1090	117	15	of	of	ADP
eurjchem-1090	117	16	the	the	DET
eurjchem-1090	117	17	mixture	mixture	NOUN
eurjchem-1090	117	18	by	by	ADP
eurjchem-1090	117	19	using	use	VERB
eurjchem-1090	117	20	only	only	ADV
eurjchem-1090	117	21	one	one	NUM
eurjchem-1090	117	22	internal	internal	ADJ
eurjchem-1090	117	23	standard	standard	NOUN
eurjchem-1090	117	24	.	.	PUNCT
eurjchem-1090	118	1	the	the	DET
eurjchem-1090	118	2	positive	positive	ADJ
eurjchem-1090	118	3	ion	ion	NOUN
eurjchem-1090	118	4	mode	mode	NOUN
eurjchem-1090	118	5	was	be	AUX
eurjchem-1090	118	6	found	find	VERB
eurjchem-1090	118	7	to	to	PART
eurjchem-1090	118	8	be	be	AUX
eurjchem-1090	118	9	the	the	DET
eurjchem-1090	118	10	most	most	ADV
eurjchem-1090	118	11	suitable	suitable	ADJ
eurjchem-1090	118	12	for	for	ADP
eurjchem-1090	118	13	the	the	DET
eurjchem-1090	118	14	lc‐tandem	lc‐tandem	PROPN
eurjchem-1090	118	15	mass	mass	PROPN
eurjchem-1090	118	16	multiple	multiple	ADJ
eurjchem-1090	118	17	reaction	reaction	NOUN
eurjchem-1090	118	18	monitoring	monitoring	NOUN
eurjchem-1090	118	19	(	(	PUNCT
eurjchem-1090	118	20	mrm	mrm	PROPN
eurjchem-1090	118	21	)	)	PUNCT
eurjchem-1090	118	22	analyses	analysis	NOUN
eurjchem-1090	118	23	.	.	PUNCT
eurjchem-1090	119	1	parent	parent	NOUN
eurjchem-1090	119	2	ion	ion	NOUN
eurjchem-1090	119	3	of	of	ADP
eurjchem-1090	119	4	each	each	DET
eurjchem-1090	119	5	analyte	analyte	NOUN
eurjchem-1090	119	6	and	and	CCONJ
eurjchem-1090	119	7	is	be	AUX
eurjchem-1090	119	8	[	[	PUNCT
eurjchem-1090	119	9	m+h]+	m+h]+	NOUN
eurjchem-1090	119	10	in	in	ADP
eurjchem-1090	119	11	the	the	DET
eurjchem-1090	119	12	first	first	ADJ
eurjchem-1090	119	13	ms	ms	NOUN
eurjchem-1090	119	14	was	be	AUX
eurjchem-1090	119	15	used	use	VERB
eurjchem-1090	119	16	to	to	PART
eurjchem-1090	119	17	give	give	VERB
eurjchem-1090	119	18	the	the	DET
eurjchem-1090	119	19	most	most	ADV
eurjchem-1090	119	20	intense	intense	ADJ
eurjchem-1090	119	21	product	product	NOUN
eurjchem-1090	119	22	ion	ion	NOUN
eurjchem-1090	119	23	peak	peak	NOUN
eurjchem-1090	119	24	in	in	ADP
eurjchem-1090	119	25	ms3	ms3	NOUN
eurjchem-1090	119	26	where	where	SCONJ
eurjchem-1090	119	27	it	it	PRON
eurjchem-1090	119	28	was	be	AUX
eurjchem-1090	119	29	used	use	VERB
eurjchem-1090	119	30	for	for	ADP
eurjchem-1090	119	31	the	the	DET
eurjchem-1090	119	32	quantitative	quantitative	ADJ
eurjchem-1090	119	33	measurement	measurement	NOUN
eurjchem-1090	119	34	.	.	PUNCT
eurjchem-1090	120	1	the	the	DET
eurjchem-1090	120	2	parent	parent	NOUN
eurjchem-1090	120	3	ion	ion	NOUN
eurjchem-1090	120	4	of	of	ADP
eurjchem-1090	120	5	the	the	DET
eurjchem-1090	120	6	protonated	protonate	VERB
eurjchem-1090	120	7	mox	mox	NOUN
eurjchem-1090	120	8	and	and	CCONJ
eurjchem-1090	120	9	moxt	moxt	NOUN
eurjchem-1090	120	10	(	(	PUNCT
eurjchem-1090	120	11	m	m	PROPN
eurjchem-1090	120	12	/	/	SYM
eurjchem-1090	120	13	z	z	PROPN
eurjchem-1090	120	14	,	,	PUNCT
eurjchem-1090	120	15	499.4	499.4	NUM
eurjchem-1090	120	16	)	)	PUNCT
eurjchem-1090	120	17	and	and	CCONJ
eurjchem-1090	120	18	(	(	PUNCT
eurjchem-1090	120	19	m	m	NOUN
eurjchem-1090	120	20	/	/	SYM
eurjchem-1090	120	21	z	z	PROPN
eurjchem-1090	120	22	,	,	PUNCT
eurjchem-1090	120	23	471	471	NUM
eurjchem-1090	120	24	)	)	PUNCT
eurjchem-1090	120	25	formed	form	VERB
eurjchem-1090	120	26	the	the	DET
eurjchem-1090	120	27	most	most	ADV
eurjchem-1090	120	28	intense	intense	ADJ
eurjchem-1090	120	29	daughter	daughter	NOUN
eurjchem-1090	120	30	ion	ion	NOUN
eurjchem-1090	120	31	peak	peak	NOUN
eurjchem-1090	120	32	at	at	ADP
eurjchem-1090	120	33	234.2	234.2	NUM
eurjchem-1090	120	34	and	and	CCONJ
eurjchem-1090	120	35	m	m	PROPN
eurjchem-1090	120	36	/	/	SYM
eurjchem-1090	120	37	z	z	NOUN
eurjchem-1090	120	38	206	206	NUM
eurjchem-1090	120	39	,	,	PUNCT
eurjchem-1090	120	40	respectively	respectively	ADV
eurjchem-1090	120	41	.	.	PUNCT
eurjchem-1090	121	1	also	also	ADV
eurjchem-1090	121	2	,	,	PUNCT
eurjchem-1090	121	3	the	the	DET
eurjchem-1090	121	4	protonated	protonate	VERB
eurjchem-1090	121	5	is	be	AUX
eurjchem-1090	121	6	(	(	PUNCT
eurjchem-1090	121	7	benz	benz	PROPN
eurjchem-1090	121	8	,	,	PUNCT
eurjchem-1090	121	9	m	m	PROPN
eurjchem-1090	121	10	/	/	SYM
eurjchem-1090	121	11	z	z	PROPN
eurjchem-1090	121	12	425.2	425.2	NUM
eurjchem-1090	121	13	)	)	PUNCT
eurjchem-1090	121	14	formed	form	VERB
eurjchem-1090	121	15	the	the	DET
eurjchem-1090	121	16	most	most	ADV
eurjchem-1090	121	17	intense	intense	ADJ
eurjchem-1090	121	18	daughter	daughter	NOUN
eurjchem-1090	121	19	ion	ion	NOUN
eurjchem-1090	121	20	peak	peak	NOUN
eurjchem-1090	121	21	at	at	ADP
eurjchem-1090	121	22	m	m	PROPN
eurjchem-1090	121	23	/	/	SYM
eurjchem-1090	121	24	z	z	PROPN
eurjchem-1090	121	25	351.2	351.2	NUM
eurjchem-1090	121	26	,	,	PUNCT
eurjchem-1090	121	27	figure	figure	NOUN
eurjchem-1090	121	28	2	2	NUM
eurjchem-1090	121	29	.	.	X
eurjchem-1090	122	1	3.1.2	3.1.2	NUM
eurjchem-1090	122	2	.	.	PUNCT
eurjchem-1090	122	3	chromatographic	chromatographic	ADJ
eurjchem-1090	122	4	conditions	condition	NOUN
eurjchem-1090	122	5	different	different	ADJ
eurjchem-1090	122	6	ratios	ratio	NOUN
eurjchem-1090	122	7	of	of	ADP
eurjchem-1090	122	8	acetonitrile	acetonitrile	NOUN
eurjchem-1090	122	9	and	and	CCONJ
eurjchem-1090	122	10	buffer	buffer	NOUN
eurjchem-1090	122	11	were	be	AUX
eurjchem-1090	122	12	tested	test	VERB
eurjchem-1090	122	13	for	for	ADP
eurjchem-1090	122	14	optimum	optimum	ADJ
eurjchem-1090	122	15	resolution	resolution	NOUN
eurjchem-1090	122	16	in	in	ADP
eurjchem-1090	122	17	a	a	DET
eurjchem-1090	122	18	reasonable	reasonable	ADJ
eurjchem-1090	122	19	run	run	NOUN
eurjchem-1090	122	20	time	time	NOUN
eurjchem-1090	122	21	and	and	CCONJ
eurjchem-1090	122	22	acceptable	acceptable	ADJ
eurjchem-1090	122	23	peak	peak	NOUN
eurjchem-1090	122	24	shape	shape	NOUN
eurjchem-1090	122	25	.	.	PUNCT
eurjchem-1090	123	1	the	the	DET
eurjchem-1090	123	2	most	most	ADV
eurjchem-1090	123	3	satisfactory	satisfactory	ADJ
eurjchem-1090	123	4	mobile	mobile	ADJ
eurjchem-1090	123	5	phase	phase	NOUN
eurjchem-1090	123	6	ratio	ratio	NOUN
eurjchem-1090	123	7	was	be	AUX
eurjchem-1090	123	8	found	find	VERB
eurjchem-1090	123	9	to	to	PART
eurjchem-1090	123	10	be	be	AUX
eurjchem-1090	123	11	0.1	0.1	NUM
eurjchem-1090	123	12	%	%	NOUN
eurjchem-1090	123	13	formic	formic	ADJ
eurjchem-1090	123	14	acid	acid	NOUN
eurjchem-1090	123	15	and	and	CCONJ
eurjchem-1090	123	16	acetonitrile	acetonitrile	NOUN
eurjchem-1090	123	17	(	(	PUNCT
eurjchem-1090	123	18	30:70	30:70	NUM
eurjchem-1090	123	19	,	,	PUNCT
eurjchem-1090	123	20	v	v	NOUN
eurjchem-1090	123	21	:	:	PUNCT
eurjchem-1090	123	22	v	v	NOUN
eurjchem-1090	123	23	)	)	PUNCT
eurjchem-1090	123	24	.	.	PUNCT
eurjchem-1090	124	1	two	two	NUM
eurjchem-1090	124	2	types	type	NOUN
eurjchem-1090	124	3	of	of	ADP
eurjchem-1090	124	4	stationary	stationary	ADJ
eurjchem-1090	124	5	phases	phase	NOUN
eurjchem-1090	124	6	c8	c8	PROPN
eurjchem-1090	124	7	and	and	CCONJ
eurjchem-1090	124	8	c18	c18	NOUN
eurjchem-1090	124	9	were	be	AUX
eurjchem-1090	124	10	investigated	investigate	VERB
eurjchem-1090	124	11	for	for	ADP
eurjchem-1090	124	12	the	the	DET
eurjchem-1090	124	13	optimum	optimum	ADJ
eurjchem-1090	124	14	resolution	resolution	NOUN
eurjchem-1090	124	15	of	of	ADP
eurjchem-1090	124	16	the	the	DET
eurjchem-1090	124	17	analytes	analyte	NOUN
eurjchem-1090	124	18	peaks	peak	NOUN
eurjchem-1090	124	19	,	,	PUNCT
eurjchem-1090	124	20	however	however	ADV
eurjchem-1090	124	21	the	the	DET
eurjchem-1090	124	22	more	more	ADV
eurjchem-1090	124	23	hydrophobic	hydrophobic	NOUN
eurjchem-1090	124	24	sunfire	sunfire	NOUN
eurjchem-1090	124	25	c18	c18	PROPN
eurjchem-1090	124	26	was	be	AUX
eurjchem-1090	124	27	found	find	VERB
eurjchem-1090	124	28	to	to	PART
eurjchem-1090	124	29	be	be	AUX
eurjchem-1090	124	30	more	more	ADV
eurjchem-1090	124	31	superior	superior	ADJ
eurjchem-1090	124	32	in	in	ADP
eurjchem-1090	124	33	separating	separate	VERB
eurjchem-1090	124	34	analytes	analyte	NOUN
eurjchem-1090	124	35	peaks	peak	NOUN
eurjchem-1090	124	36	in	in	ADP
eurjchem-1090	124	37	a	a	DET
eurjchem-1090	124	38	reasonable	reasonable	ADJ
eurjchem-1090	124	39	run	run	NOUN
eurjchem-1090	124	40	time	time	NOUN
eurjchem-1090	124	41	.	.	PUNCT
eurjchem-1090	125	1	3.1.3	3.1.3	NUM
eurjchem-1090	125	2	.	.	NOUN
eurjchem-1090	125	3	simple	simple	ADJ
eurjchem-1090	125	4	protein	protein	NOUN
eurjchem-1090	125	5	precipitation	precipitation	NOUN
eurjchem-1090	125	6	simple	simple	ADJ
eurjchem-1090	125	7	protein	protein	NOUN
eurjchem-1090	125	8	precipitation	precipitation	NOUN
eurjchem-1090	125	9	was	be	AUX
eurjchem-1090	125	10	used	use	VERB
eurjchem-1090	125	11	to	to	PART
eurjchem-1090	125	12	obtain	obtain	VERB
eurjchem-1090	125	13	samples	sample	NOUN
eurjchem-1090	125	14	free	free	ADJ
eurjchem-1090	125	15	from	from	ADP
eurjchem-1090	125	16	endogenous	endogenous	ADJ
eurjchem-1090	125	17	interferents	interferent	NOUN
eurjchem-1090	125	18	,	,	PUNCT
eurjchem-1090	125	19	which	which	PRON
eurjchem-1090	125	20	are	be	AUX
eurjchem-1090	125	21	essential	essential	ADJ
eurjchem-1090	125	22	for	for	ADP
eurjchem-1090	125	23	increasing	increase	VERB
eurjchem-1090	125	24	recovery	recovery	NOUN
eurjchem-1090	125	25	and	and	CCONJ
eurjchem-1090	125	26	minimizing	minimize	VERB
eurjchem-1090	125	27	matrix	matrix	NOUN
eurjchem-1090	125	28	effects	effect	NOUN
eurjchem-1090	125	29	in	in	ADP
eurjchem-1090	125	30	lc‐	lc‐	ADJ
eurjchem-1090	125	31	tandem	tandem	NOUN
eurjchem-1090	125	32	mass	mass	PROPN
eurjchem-1090	125	33	spectrometry	spectrometry	NOUN
eurjchem-1090	125	34	.	.	PUNCT
eurjchem-1090	126	1	different	different	ADJ
eurjchem-1090	126	2	precipitating	precipitating	NOUN
eurjchem-1090	126	3	solvents	solvent	NOUN
eurjchem-1090	126	4	,	,	PUNCT
eurjchem-1090	126	5	like	like	ADP
eurjchem-1090	126	6	methanol	methanol	NOUN
eurjchem-1090	126	7	,	,	PUNCT
eurjchem-1090	126	8	and	and	CCONJ
eurjchem-1090	126	9	acetonitrile	acetonitrile	NOUN
eurjchem-1090	126	10	were	be	AUX
eurjchem-1090	126	11	tried	try	VERB
eurjchem-1090	126	12	and	and	CCONJ
eurjchem-1090	126	13	tested	test	VERB
eurjchem-1090	126	14	for	for	ADP
eurjchem-1090	126	15	removing	remove	VERB
eurjchem-1090	126	16	interferents	interferent	NOUN
eurjchem-1090	126	17	and	and	CCONJ
eurjchem-1090	126	18	obtaining	obtain	VERB
eurjchem-1090	126	19	clean	clean	ADJ
eurjchem-1090	126	20	plasma	plasma	NOUN
eurjchem-1090	126	21	samples	sample	NOUN
eurjchem-1090	126	22	leading	lead	VERB
eurjchem-1090	126	23	to	to	ADP
eurjchem-1090	126	24	acceptable	acceptable	ADJ
eurjchem-1090	126	25	matrix	matrix	NOUN
eurjchem-1090	126	26	effect	effect	NOUN
eurjchem-1090	126	27	and	and	CCONJ
eurjchem-1090	126	28	recoveries	recovery	NOUN
eurjchem-1090	126	29	.	.	PUNCT
eurjchem-1090	127	1	acetonitrile	acetonitrile	NOUN
eurjchem-1090	127	2	proved	prove	VERB
eurjchem-1090	127	3	to	to	PART
eurjchem-1090	127	4	be	be	AUX
eurjchem-1090	127	5	the	the	DET
eurjchem-1090	127	6	most	most	ADV
eurjchem-1090	127	7	suitable	suitable	ADJ
eurjchem-1090	127	8	,	,	PUNCT
eurjchem-1090	127	9	so	so	SCONJ
eurjchem-1090	127	10	it	it	PRON
eurjchem-1090	127	11	was	be	AUX
eurjchem-1090	127	12	used	use	VERB
eurjchem-1090	127	13	in	in	ADP
eurjchem-1090	127	14	the	the	DET
eurjchem-1090	127	15	protein	protein	NOUN
eurjchem-1090	127	16	precipitation	precipitation	NOUN
eurjchem-1090	127	17	step	step	NOUN
eurjchem-1090	127	18	.	.	PUNCT
eurjchem-1090	128	1	3.1.4	3.1.4	NUM
eurjchem-1090	128	2	.	.	PUNCT
eurjchem-1090	128	3	selection	selection	NOUN
eurjchem-1090	128	4	of	of	ADP
eurjchem-1090	128	5	internal	internal	ADJ
eurjchem-1090	128	6	standard	standard	ADJ
eurjchem-1090	128	7	internal	internal	ADJ
eurjchem-1090	128	8	standard	standard	NOUN
eurjchem-1090	128	9	(	(	PUNCT
eurjchem-1090	128	10	is	be	AUX
eurjchem-1090	128	11	)	)	PUNCT
eurjchem-1090	128	12	is	be	AUX
eurjchem-1090	128	13	used	use	VERB
eurjchem-1090	128	14	to	to	PART
eurjchem-1090	128	15	compensate	compensate	VERB
eurjchem-1090	128	16	for	for	ADP
eurjchem-1090	128	17	the	the	DET
eurjchem-1090	128	18	analytes	analyte	NOUN
eurjchem-1090	128	19	during	during	ADP
eurjchem-1090	128	20	any	any	DET
eurjchem-1090	128	21	step	step	NOUN
eurjchem-1090	128	22	of	of	ADP
eurjchem-1090	128	23	the	the	DET
eurjchem-1090	128	24	analysis	analysis	NOUN
eurjchem-1090	128	25	.	.	PUNCT
eurjchem-1090	129	1	also	also	ADV
eurjchem-1090	129	2	,	,	PUNCT
eurjchem-1090	129	3	matrix	matrix	NOUN
eurjchem-1090	129	4	effect	effect	NOUN
eurjchem-1090	129	5	could	could	AUX
eurjchem-1090	129	6	be	be	AUX
eurjchem-1090	129	7	minimized	minimize	VERB
eurjchem-1090	129	8	by	by	ADP
eurjchem-1090	129	9	choosing	choose	VERB
eurjchem-1090	129	10	suitable	suitable	ADJ
eurjchem-1090	129	11	is	be	AUX
eurjchem-1090	129	12	.	.	PUNCT
eurjchem-1090	130	1	several	several	ADJ
eurjchem-1090	130	2	compounds	compound	NOUN
eurjchem-1090	130	3	were	be	AUX
eurjchem-1090	130	4	investigated	investigate	VERB
eurjchem-1090	130	5	,	,	PUNCT
eurjchem-1090	130	6	such	such	ADJ
eurjchem-1090	130	7	as	as	ADP
eurjchem-1090	130	8	torasemid	torasemid	NOUN
eurjchem-1090	130	9	,	,	PUNCT
eurjchem-1090	130	10	gliclazide	gliclazide	NOUN
eurjchem-1090	130	11	,	,	PUNCT
eurjchem-1090	130	12	and	and	CCONJ
eurjchem-1090	130	13	benz	benz	PROPN
eurjchem-1090	130	14	,	,	PUNCT
eurjchem-1090	130	15	and	and	CCONJ
eurjchem-1090	130	16	finally	finally	ADV
eurjchem-1090	130	17	benz	benz	PROPN
eurjchem-1090	130	18	was	be	AUX
eurjchem-1090	130	19	found	find	VERB
eurjchem-1090	130	20	to	to	PART
eurjchem-1090	130	21	be	be	AUX
eurjchem-1090	130	22	the	the	DET
eurjchem-1090	130	23	most	most	ADV
eurjchem-1090	130	24	suitable	suitable	ADJ
eurjchem-1090	130	25	is	be	AUX
eurjchem-1090	130	26	.	.	PUNCT
eurjchem-1090	131	1	3.2	3.2	NUM
eurjchem-1090	131	2	.	.	PUNCT
eurjchem-1090	131	3	method	method	NOUN
eurjchem-1090	131	4	validation	validation	NOUN
eurjchem-1090	131	5	3.2.1	3.2.1	NUM
eurjchem-1090	131	6	.	.	PUNCT
eurjchem-1090	132	1	selectivity	selectivity	NOUN
eurjchem-1090	132	2	to	to	PART
eurjchem-1090	132	3	test	test	VERB
eurjchem-1090	132	4	for	for	ADP
eurjchem-1090	132	5	the	the	DET
eurjchem-1090	132	6	method	method	NOUN
eurjchem-1090	132	7	selectivity	selectivity	NOUN
eurjchem-1090	132	8	,	,	PUNCT
eurjchem-1090	132	9	blank	blank	ADJ
eurjchem-1090	132	10	plasma	plasma	NOUN
eurjchem-1090	132	11	samples	sample	NOUN
eurjchem-1090	132	12	from	from	ADP
eurjchem-1090	132	13	six	six	NUM
eurjchem-1090	132	14	different	different	ADJ
eurjchem-1090	132	15	sources	source	NOUN
eurjchem-1090	132	16	were	be	AUX
eurjchem-1090	132	17	analyzed	analyze	VERB
eurjchem-1090	132	18	to	to	PART
eurjchem-1090	132	19	be	be	AUX
eurjchem-1090	132	20	sure	sure	ADJ
eurjchem-1090	132	21	that	that	SCONJ
eurjchem-1090	132	22	the	the	DET
eurjchem-1090	132	23	endogenous	endogenous	ADJ
eurjchem-1090	132	24	plasma	plasma	NOUN
eurjchem-1090	132	25	constituents	constituent	NOUN
eurjchem-1090	132	26	show	show	VERB
eurjchem-1090	132	27	no	no	DET
eurjchem-1090	132	28	interference	interference	NOUN
eurjchem-1090	132	29	at	at	ADP
eurjchem-1090	132	30	the	the	DET
eurjchem-1090	132	31	peak	peak	NOUN
eurjchem-1090	132	32	region	region	NOUN
eurjchem-1090	132	33	of	of	ADP
eurjchem-1090	132	34	the	the	DET
eurjchem-1090	132	35	studied	study	VERB
eurjchem-1090	132	36	analytes	analyte	NOUN
eurjchem-1090	132	37	and	and	CCONJ
eurjchem-1090	132	38	the	the	PRON
eurjchem-1090	132	39	is	be	AUX
eurjchem-1090	132	40	.	.	PUNCT
eurjchem-1090	133	1	the	the	DET
eurjchem-1090	133	2	proposed	propose	VERB
eurjchem-1090	133	3	method	method	NOUN
eurjchem-1090	133	4	showed	show	VERB
eurjchem-1090	133	5	no	no	DET
eurjchem-1090	133	6	interference	interference	NOUN
eurjchem-1090	133	7	at	at	ADP
eurjchem-1090	133	8	the	the	DET
eurjchem-1090	133	9	m	m	PROPN
eurjchem-1090	133	10	/	/	SYM
eurjchem-1090	133	11	z	z	NOUN
eurjchem-1090	133	12	ratio	ratio	NOUN
eurjchem-1090	133	13	of	of	ADP
eurjchem-1090	133	14	the	the	DET
eurjchem-1090	133	15	analytes	analyte	NOUN
eurjchem-1090	133	16	and	and	CCONJ
eurjchem-1090	133	17	is	be	AUX
eurjchem-1090	133	18	,	,	PUNCT
eurjchem-1090	133	19	figure	figure	NOUN
eurjchem-1090	133	20	3‐5	3‐5	NUM
eurjchem-1090	133	21	.	.	PUNCT
eurjchem-1090	134	1	3.2.2	3.2.2	NUM
eurjchem-1090	134	2	.	.	PUNCT
eurjchem-1090	135	1	lower	low	ADJ
eurjchem-1090	135	2	limit	limit	NOUN
eurjchem-1090	135	3	of	of	ADP
eurjchem-1090	135	4	the	the	DET
eurjchem-1090	135	5	quantitation	quantitation	NOUN
eurjchem-1090	135	6	(	(	PUNCT
eurjchem-1090	135	7	lloq	lloq	PROPN
eurjchem-1090	135	8	)	)	PUNCT
eurjchem-1090	135	9	the	the	DET
eurjchem-1090	135	10	lloq	lloq	NOUN
eurjchem-1090	135	11	was	be	AUX
eurjchem-1090	135	12	defined	define	VERB
eurjchem-1090	135	13	as	as	ADP
eurjchem-1090	135	14	the	the	DET
eurjchem-1090	135	15	lowest	low	ADJ
eurjchem-1090	135	16	concentration	concentration	NOUN
eurjchem-1090	135	17	on	on	ADP
eurjchem-1090	135	18	the	the	DET
eurjchem-1090	135	19	calibration	calibration	NOUN
eurjchem-1090	135	20	curves	curve	NOUN
eurjchem-1090	135	21	with	with	ADP
eurjchem-1090	135	22	acceptable	acceptable	ADJ
eurjchem-1090	135	23	precision	precision	NOUN
eurjchem-1090	135	24	and	and	CCONJ
eurjchem-1090	135	25	recovery	recovery	NOUN
eurjchem-1090	135	26	.	.	PUNCT
eurjchem-1090	136	1	elaziz	elaziz	PROPN
eurjchem-1090	136	2	et	et	PROPN
eurjchem-1090	136	3	al	al	PROPN
eurjchem-1090	136	4	.	.	PUNCT
eurjchem-1090	136	5	/	/	SYM
eurjchem-1090	136	6	european	european	PROPN
eurjchem-1090	136	7	journal	journal	PROPN
eurjchem-1090	136	8	of	of	ADP
eurjchem-1090	136	9	chemistry	chemistry	NOUN
eurjchem-1090	136	10	5	5	NUM
eurjchem-1090	136	11	(	(	PUNCT
eurjchem-1090	136	12	4	4	NUM
eurjchem-1090	136	13	)	)	PUNCT
eurjchem-1090	136	14	(	(	PUNCT
eurjchem-1090	136	15	2014	2014	NUM
eurjchem-1090	136	16	)	)	PUNCT
eurjchem-1090	136	17	662‐667	662‐667	NUM
eurjchem-1090	136	18	665	665	NUM
eurjchem-1090	136	19	table	table	NOUN
eurjchem-1090	136	20	1	1	NUM
eurjchem-1090	136	21	.	.	PUNCT
eurjchem-1090	137	1	the	the	DET
eurjchem-1090	137	2	recovery	recovery	NOUN
eurjchem-1090	137	3	and	and	CCONJ
eurjchem-1090	137	4	matrix	matrix	NOUN
eurjchem-1090	137	5	effect	effect	NOUN
eurjchem-1090	137	6	of	of	ADP
eurjchem-1090	137	7	moexipril	moexipril	NOUN
eurjchem-1090	137	8	,	,	PUNCT
eurjchem-1090	137	9	moexiprilat	moexiprilat	NOUN
eurjchem-1090	137	10	,	,	PUNCT
eurjchem-1090	137	11	and	and	CCONJ
eurjchem-1090	137	12	is	be	AUX
eurjchem-1090	137	13	(	(	PUNCT
eurjchem-1090	137	14	n	n	NOUN
eurjchem-1090	137	15	=	=	SYM
eurjchem-1090	137	16	3	3	NUM
eurjchem-1090	137	17	)	)	PUNCT
eurjchem-1090	137	18	.	.	PUNCT
eurjchem-1090	138	1	analyte	analyte	NOUN
eurjchem-1090	138	2	c	c	PROPN
eurjchem-1090	138	3	(	(	PUNCT
eurjchem-1090	138	4	ng	ng	PROPN
eurjchem-1090	138	5	/	/	SYM
eurjchem-1090	138	6	ml	ml	NOUN
eurjchem-1090	138	7	)	)	PUNCT
eurjchem-1090	138	8	recovery	recovery	NOUN
eurjchem-1090	138	9	(	(	PUNCT
eurjchem-1090	138	10	%	%	NOUN
eurjchem-1090	138	11	)	)	PUNCT
eurjchem-1090	138	12	matrix	matrix	NOUN
eurjchem-1090	138	13	effect	effect	NOUN
eurjchem-1090	138	14	(	(	PUNCT
eurjchem-1090	138	15	%	%	INTJ
eurjchem-1090	138	16	)	)	PUNCT
eurjchem-1090	139	1	x±sd	x±sd	PUNCT
eurjchem-1090	139	2	rsd	rsd	PROPN
eurjchem-1090	139	3	%	%	NOUN
eurjchem-1090	139	4	x±sd	x±sd	PUNCT
eurjchem-1090	140	1	rsd	rsd	PROPN
eurjchem-1090	140	2	%	%	NOUN
eurjchem-1090	140	3	moexipril	moexipril	NOUN
eurjchem-1090	140	4	15	15	NUM
eurjchem-1090	140	5	84.6±3.87	84.6±3.87	NUM
eurjchem-1090	140	6	4.57	4.57	NUM
eurjchem-1090	140	7	99.7±2.45	99.7±2.45	NUM
eurjchem-1090	140	8	2.46	2.46	NUM
eurjchem-1090	140	9	50	50	NUM
eurjchem-1090	140	10	83.7±5.41	83.7±5.41	NUM
eurjchem-1090	140	11	6.46	6.46	NUM
eurjchem-1090	140	12	98.3±1.48	98.3±1.48	NUM
eurjchem-1090	140	13	1.50	1.50	NUM
eurjchem-1090	140	14	180	180	NUM
eurjchem-1090	140	15	84.6±5.23	84.6±5.23	NUM
eurjchem-1090	140	16	6.18	6.18	NUM
eurjchem-1090	140	17	98.7±1.62	98.7±1.62	NUM
eurjchem-1090	140	18	1.64	1.64	NUM
eurjchem-1090	140	19	moexiprilat	moexiprilat	NOUN
eurjchem-1090	140	20	3	3	NUM
eurjchem-1090	140	21	86.5±4.84	86.5±4.84	NUM
eurjchem-1090	140	22	5.60	5.60	NUM
eurjchem-1090	140	23	98.9±2.16	98.9±2.16	NUM
eurjchem-1090	140	24	2.18	2.18	NUM
eurjchem-1090	140	25	30	30	NUM
eurjchem-1090	140	26	85.1±8.64	85.1±8.64	NUM
eurjchem-1090	140	27	10.15	10.15	NUM
eurjchem-1090	140	28	99.5±3.12	99.5±3.12	NUM
eurjchem-1090	140	29	3.14	3.14	NUM
eurjchem-1090	140	30	100	100	NUM
eurjchem-1090	140	31	85.5±2.47	85.5±2.47	NUM
eurjchem-1090	140	32	2.89	2.89	NUM
eurjchem-1090	140	33	99.4±1.57	99.4±1.57	NUM
eurjchem-1090	140	34	1.58	1.58	NUM
eurjchem-1090	140	35	is	be	AUX
eurjchem-1090	140	36	10	10	NUM
eurjchem-1090	140	37	87.3±4.57	87.3±4.57	NUM
eurjchem-1090	140	38	5.23	5.23	NUM
eurjchem-1090	140	39	99.7±2.47	99.7±2.47	NUM
eurjchem-1090	140	40	2.48	2.48	NUM
eurjchem-1090	140	41	(	(	PUNCT
eurjchem-1090	140	42	a	a	NOUN
eurjchem-1090	140	43	)	)	PUNCT
eurjchem-1090	140	44	(	(	PUNCT
eurjchem-1090	140	45	b	b	X
eurjchem-1090	140	46	)	)	PUNCT
eurjchem-1090	140	47	(	(	PUNCT
eurjchem-1090	140	48	c	c	X
eurjchem-1090	140	49	)	)	PUNCT
eurjchem-1090	140	50	figure	figure	NOUN
eurjchem-1090	140	51	2	2	NUM
eurjchem-1090	140	52	.	.	PUNCT
eurjchem-1090	141	1	ms	ms	PROPN
eurjchem-1090	141	2	spectra	spectra	PROPN
eurjchem-1090	141	3	for	for	ADP
eurjchem-1090	141	4	(	(	PUNCT
eurjchem-1090	141	5	a	a	PRON
eurjchem-1090	141	6	)	)	PUNCT
eurjchem-1090	141	7	moexipril	moexipril	NOUN
eurjchem-1090	141	8	,	,	PUNCT
eurjchem-1090	141	9	(	(	PUNCT
eurjchem-1090	141	10	b	b	NOUN
eurjchem-1090	141	11	)	)	PUNCT
eurjchem-1090	141	12	moexiprilat	moexiprilat	NOUN
eurjchem-1090	141	13	,	,	PUNCT
eurjchem-1090	141	14	and	and	CCONJ
eurjchem-1090	141	15	(	(	PUNCT
eurjchem-1090	141	16	c	c	X
eurjchem-1090	141	17	)	)	PUNCT
eurjchem-1090	141	18	benazepril	benazepril	NOUN
eurjchem-1090	141	19	.	.	PUNCT
eurjchem-1090	142	1	the	the	DET
eurjchem-1090	142	2	analyte	analyte	NOUN
eurjchem-1090	142	3	response	response	NOUN
eurjchem-1090	142	4	at	at	ADP
eurjchem-1090	142	5	the	the	DET
eurjchem-1090	142	6	lloq	lloq	NOUN
eurjchem-1090	142	7	should	should	AUX
eurjchem-1090	142	8	be	be	AUX
eurjchem-1090	142	9	at	at	ADV
eurjchem-1090	142	10	least	least	ADV
eurjchem-1090	142	11	five	five	NUM
eurjchem-1090	142	12	times	time	NOUN
eurjchem-1090	142	13	the	the	DET
eurjchem-1090	142	14	response	response	NOUN
eurjchem-1090	142	15	of	of	ADP
eurjchem-1090	142	16	blank	blank	ADJ
eurjchem-1090	142	17	baseline	baseline	NOUN
eurjchem-1090	142	18	.	.	PUNCT
eurjchem-1090	143	1	to	to	PART
eurjchem-1090	143	2	test	test	VERB
eurjchem-1090	143	3	for	for	ADP
eurjchem-1090	143	4	lloq	lloq	NOUN
eurjchem-1090	143	5	of	of	ADP
eurjchem-1090	143	6	the	the	DET
eurjchem-1090	143	7	proposed	propose	VERB
eurjchem-1090	143	8	method	method	NOUN
eurjchem-1090	143	9	,	,	PUNCT
eurjchem-1090	143	10	three	three	NUM
eurjchem-1090	143	11	replicates	replicate	NOUN
eurjchem-1090	143	12	of	of	ADP
eurjchem-1090	143	13	the	the	DET
eurjchem-1090	143	14	spiked	spiked	ADJ
eurjchem-1090	143	15	plasma	plasma	NOUN
eurjchem-1090	143	16	samples	sample	NOUN
eurjchem-1090	143	17	were	be	AUX
eurjchem-1090	143	18	analyzed	analyze	VERB
eurjchem-1090	143	19	at	at	ADP
eurjchem-1090	143	20	concentrations	concentration	NOUN
eurjchem-1090	143	21	of	of	ADP
eurjchem-1090	143	22	0.5	0.5	NUM
eurjchem-1090	143	23	and	and	CCONJ
eurjchem-1090	143	24	5.0	5.0	NUM
eurjchem-1090	143	25	ng	ng	NOUN
eurjchem-1090	143	26	/	/	SYM
eurjchem-1090	143	27	ml	ml	X
eurjchem-1090	143	28	for	for	ADP
eurjchem-1090	143	29	mox	mox	NOUN
eurjchem-1090	143	30	and	and	CCONJ
eurjchem-1090	143	31	moxt	moxt	NOUN
eurjchem-1090	143	32	,	,	PUNCT
eurjchem-1090	143	33	respectively	respectively	ADV
eurjchem-1090	143	34	.	.	PUNCT
eurjchem-1090	144	1	the	the	DET
eurjchem-1090	144	2	precision	precision	NOUN
eurjchem-1090	144	3	and	and	CCONJ
eurjchem-1090	144	4	accuracy	accuracy	NOUN
eurjchem-1090	144	5	were	be	AUX
eurjchem-1090	144	6	found	find	VERB
eurjchem-1090	144	7	to	to	PART
eurjchem-1090	144	8	be	be	AUX
eurjchem-1090	144	9	5.09	5.09	NUM
eurjchem-1090	144	10	and	and	CCONJ
eurjchem-1090	144	11	102	102	NUM
eurjchem-1090	144	12	%	%	NOUN
eurjchem-1090	144	13	for	for	ADP
eurjchem-1090	144	14	mox	mox	NOUN
eurjchem-1090	144	15	;	;	PUNCT
eurjchem-1090	144	16	0.97	0.97	NUM
eurjchem-1090	144	17	and	and	CCONJ
eurjchem-1090	144	18	104	104	NUM
eurjchem-1090	144	19	%	%	NOUN
eurjchem-1090	144	20	for	for	ADP
eurjchem-1090	144	21	moxt	moxt	NOUN
eurjchem-1090	144	22	,	,	PUNCT
eurjchem-1090	144	23	respectively	respectively	ADV
eurjchem-1090	144	24	.	.	PUNCT
eurjchem-1090	145	1	3.2.3	3.2.3	X
eurjchem-1090	145	2	.	.	X
eurjchem-1090	145	3	recovery	recovery	NOUN
eurjchem-1090	145	4	and	and	CCONJ
eurjchem-1090	145	5	matrix	matrix	NOUN
eurjchem-1090	145	6	effect	effect	NOUN
eurjchem-1090	145	7	different	different	ADJ
eurjchem-1090	145	8	precipitating	precipitating	NOUN
eurjchem-1090	145	9	solvents	solvent	NOUN
eurjchem-1090	145	10	were	be	AUX
eurjchem-1090	145	11	tried	try	VERB
eurjchem-1090	145	12	to	to	PART
eurjchem-1090	145	13	obtain	obtain	VERB
eurjchem-1090	145	14	clean	clean	ADJ
eurjchem-1090	145	15	samples	sample	NOUN
eurjchem-1090	145	16	,	,	PUNCT
eurjchem-1090	145	17	minimize	minimize	VERB
eurjchem-1090	145	18	matrix	matrix	NOUN
eurjchem-1090	145	19	effect	effect	NOUN
eurjchem-1090	145	20	,	,	PUNCT
eurjchem-1090	145	21	and	and	CCONJ
eurjchem-1090	145	22	increase	increase	VERB
eurjchem-1090	145	23	recovery	recovery	NOUN
eurjchem-1090	145	24	%	%	NOUN
eurjchem-1090	145	25	.	.	PUNCT
eurjchem-1090	146	1	acetonitrile	acetonitrile	PROPN
eurjchem-1090	146	2	proved	prove	VERB
eurjchem-1090	146	3	to	to	PART
eurjchem-1090	146	4	be	be	AUX
eurjchem-1090	146	5	the	the	DET
eurjchem-1090	146	6	most	most	ADV
eurjchem-1090	146	7	suitable	suitable	ADJ
eurjchem-1090	146	8	one	one	NUM
eurjchem-1090	146	9	for	for	ADP
eurjchem-1090	146	10	extraction	extraction	NOUN
eurjchem-1090	146	11	.	.	PUNCT
eurjchem-1090	147	1	the	the	DET
eurjchem-1090	147	2	recoveries	recovery	NOUN
eurjchem-1090	147	3	and	and	CCONJ
eurjchem-1090	147	4	matrix	matrix	NOUN
eurjchem-1090	147	5	effects	effect	NOUN
eurjchem-1090	147	6	of	of	ADP
eurjchem-1090	147	7	mox	mox	NOUN
eurjchem-1090	147	8	,	,	PUNCT
eurjchem-1090	147	9	moxt	moxt	NOUN
eurjchem-1090	147	10	,	,	PUNCT
eurjchem-1090	147	11	and	and	CCONJ
eurjchem-1090	147	12	benz	benz	PROPN
eurjchem-1090	147	13	(	(	PUNCT
eurjchem-1090	147	14	is	be	AUX
eurjchem-1090	147	15	)	)	PUNCT
eurjchem-1090	147	16	are	be	AUX
eurjchem-1090	147	17	shown	show	VERB
eurjchem-1090	147	18	in	in	ADP
eurjchem-1090	147	19	table	table	NOUN
eurjchem-1090	147	20	1	1	NUM
eurjchem-1090	147	21	.	.	PUNCT
eurjchem-1090	147	22	where	where	SCONJ
eurjchem-1090	147	23	three	three	NUM
eurjchem-1090	147	24	quality	quality	NOUN
eurjchem-1090	147	25	control	control	NOUN
eurjchem-1090	147	26	levels	level	NOUN
eurjchem-1090	147	27	were	be	AUX
eurjchem-1090	147	28	tested	test	VERB
eurjchem-1090	147	29	in	in	ADP
eurjchem-1090	147	30	triplicates	triplicate	NOUN
eurjchem-1090	147	31	.	.	PUNCT
eurjchem-1090	148	1	3.2.4	3.2.4	NUM
eurjchem-1090	148	2	.	.	PUNCT
eurjchem-1090	149	1	linearity	linearity	NOUN
eurjchem-1090	149	2	the	the	DET
eurjchem-1090	149	3	two	two	NUM
eurjchem-1090	149	4	analytes	analyte	NOUN
eurjchem-1090	149	5	showed	show	VERB
eurjchem-1090	149	6	linear	linear	ADJ
eurjchem-1090	149	7	response	response	NOUN
eurjchem-1090	149	8	where	where	SCONJ
eurjchem-1090	149	9	the	the	DET
eurjchem-1090	149	10	correlation	correlation	NOUN
eurjchem-1090	149	11	coefficients	coefficient	VERB
eurjchem-1090	149	12	(	(	PUNCT
eurjchem-1090	149	13	r2	r2	PROPN
eurjchem-1090	149	14	)	)	PUNCT
eurjchem-1090	149	15	were	be	AUX
eurjchem-1090	149	16	all	all	PRON
eurjchem-1090	149	17	>	>	X
eurjchem-1090	149	18	0.998	0.998	NUM
eurjchem-1090	149	19	.	.	PUNCT
eurjchem-1090	150	1	the	the	DET
eurjchem-1090	150	2	equation	equation	NOUN
eurjchem-1090	150	3	of	of	ADP
eurjchem-1090	150	4	each	each	DET
eurjchem-1090	150	5	calibration	calibration	NOUN
eurjchem-1090	150	6	curve	curve	NOUN
eurjchem-1090	150	7	was	be	AUX
eurjchem-1090	150	8	:	:	PUNCT
eurjchem-1090	150	9	y	y	PROPN
eurjchem-1090	150	10	=	=	SYM
eurjchem-1090	150	11	0.0068x	0.0068x	NUM
eurjchem-1090	150	12	‐	‐	NOUN
eurjchem-1090	150	13	0.0072	0.0072	NUM
eurjchem-1090	150	14	(	(	PUNCT
eurjchem-1090	150	15	r2	r2	NOUN
eurjchem-1090	150	16	=	=	PUNCT
eurjchem-1090	150	17	0.9981	0.9981	NUM
eurjchem-1090	150	18	,	,	PUNCT
eurjchem-1090	150	19	n	n	NOUN
eurjchem-1090	150	20	=	=	SYM
eurjchem-1090	150	21	3	3	NUM
eurjchem-1090	150	22	)	)	PUNCT
eurjchem-1090	150	23	for	for	ADP
eurjchem-1090	150	24	mox	mox	NOUN
eurjchem-1090	150	25	and	and	CCONJ
eurjchem-1090	150	26	y	y	NOUN
eurjchem-1090	150	27	=	=	SYM
eurjchem-1090	150	28	0.6098x‐0.135	0.6098x‐0.135	NOUN
eurjchem-1090	150	29	(	(	PUNCT
eurjchem-1090	150	30	r2	r2	PROPN
eurjchem-1090	150	31	=	=	SYM
eurjchem-1090	150	32	0.9988	0.9988	NUM
eurjchem-1090	150	33	,	,	PUNCT
eurjchem-1090	150	34	n	n	NOUN
eurjchem-1090	150	35	=	=	SYM
eurjchem-1090	150	36	3	3	NUM
eurjchem-1090	150	37	)	)	PUNCT
eurjchem-1090	150	38	for	for	ADP
eurjchem-1090	150	39	moxt	moxt	NOUN
eurjchem-1090	150	40	.	.	PUNCT
eurjchem-1090	151	1	3.2.5	3.2.5	X
eurjchem-1090	151	2	.	.	X
eurjchem-1090	151	3	precision	precision	NOUN
eurjchem-1090	151	4	and	and	CCONJ
eurjchem-1090	151	5	accuracy	accuracy	NOUN
eurjchem-1090	151	6	intra‐	intra‐	PROPN
eurjchem-1090	151	7	and	and	CCONJ
eurjchem-1090	151	8	inter‐day	inter‐day	PROPN
eurjchem-1090	151	9	precision	precision	NOUN
eurjchem-1090	151	10	and	and	CCONJ
eurjchem-1090	151	11	accuracy	accuracy	NOUN
eurjchem-1090	151	12	data	datum	NOUN
eurjchem-1090	151	13	for	for	ADP
eurjchem-1090	151	14	plasma	plasma	NOUN
eurjchem-1090	151	15	samples	sample	NOUN
eurjchem-1090	151	16	of	of	ADP
eurjchem-1090	151	17	the	the	DET
eurjchem-1090	151	18	two	two	NUM
eurjchem-1090	151	19	analytes	analyte	NOUN
eurjchem-1090	151	20	are	be	AUX
eurjchem-1090	151	21	shown	show	VERB
eurjchem-1090	151	22	in	in	ADP
eurjchem-1090	151	23	table	table	NOUN
eurjchem-1090	151	24	2	2	NUM
eurjchem-1090	151	25	.	.	PUNCT
eurjchem-1090	152	1	the	the	DET
eurjchem-1090	152	2	data	datum	NOUN
eurjchem-1090	152	3	showed	show	VERB
eurjchem-1090	152	4	acceptable	acceptable	ADJ
eurjchem-1090	152	5	results	result	NOUN
eurjchem-1090	152	6	for	for	ADP
eurjchem-1090	152	7	both	both	DET
eurjchem-1090	152	8	precision	precision	NOUN
eurjchem-1090	152	9	and	and	CCONJ
eurjchem-1090	152	10	accuracy	accuracy	NOUN
eurjchem-1090	152	11	.	.	PUNCT
eurjchem-1090	153	1	3.2.6	3.2.6	X
eurjchem-1090	153	2	.	.	PUNCT
eurjchem-1090	154	1	stability	stability	NOUN
eurjchem-1090	154	2	studies	study	VERB
eurjchem-1090	154	3	666	666	NUM
eurjchem-1090	154	4	elaziz	elaziz	PROPN
eurjchem-1090	154	5	et	et	PROPN
eurjchem-1090	154	6	al	al	PROPN
eurjchem-1090	154	7	.	.	PUNCT
eurjchem-1090	154	8	/	/	SYM
eurjchem-1090	154	9	european	european	PROPN
eurjchem-1090	154	10	journal	journal	PROPN
eurjchem-1090	154	11	of	of	ADP
eurjchem-1090	154	12	chemistry	chemistry	NOUN
eurjchem-1090	154	13	5	5	NUM
eurjchem-1090	154	14	(	(	PUNCT
eurjchem-1090	154	15	4	4	NUM
eurjchem-1090	154	16	)	)	PUNCT
eurjchem-1090	154	17	(	(	PUNCT
eurjchem-1090	154	18	2014	2014	NUM
eurjchem-1090	154	19	)	)	PUNCT
eurjchem-1090	154	20	662‐667	662‐667	NUM
eurjchem-1090	154	21	table	table	NOUN
eurjchem-1090	154	22	2	2	NUM
eurjchem-1090	154	23	.	.	PUNCT
eurjchem-1090	155	1	the	the	DET
eurjchem-1090	155	2	intra‐day	intra‐day	NOUN
eurjchem-1090	155	3	and	and	CCONJ
eurjchem-1090	155	4	inter‐day	inter‐day	NOUN
eurjchem-1090	155	5	precisions	precision	NOUN
eurjchem-1090	155	6	and	and	CCONJ
eurjchem-1090	155	7	accuracy	accuracy	NOUN
eurjchem-1090	155	8	of	of	ADP
eurjchem-1090	155	9	moexipril	moexipril	NOUN
eurjchem-1090	155	10	and	and	CCONJ
eurjchem-1090	155	11	moexiprilat	moexiprilat	NOUN
eurjchem-1090	155	12	in	in	ADP
eurjchem-1090	155	13	plasma	plasma	NOUN
eurjchem-1090	155	14	(	(	PUNCT
eurjchem-1090	155	15	n	n	NOUN
eurjchem-1090	155	16	=	=	SYM
eurjchem-1090	155	17	3	3	NUM
eurjchem-1090	155	18	)	)	PUNCT
eurjchem-1090	155	19	.	.	PUNCT
eurjchem-1090	156	1	analyte	analyte	NOUN
eurjchem-1090	156	2	c	c	PROPN
eurjchem-1090	156	3	(	(	PUNCT
eurjchem-1090	156	4	ng	ng	PROPN
eurjchem-1090	156	5	/	/	SYM
eurjchem-1090	156	6	ml	ml	NOUN
eurjchem-1090	156	7	)	)	PUNCT
eurjchem-1090	156	8	intra‐day	intra‐day	PROPN
eurjchem-1090	156	9	inter‐day	inter‐day	PROPN
eurjchem-1090	156	10	x±sd	x±sd	PROPN
eurjchem-1090	156	11	accuracy	accuracy	NOUN
eurjchem-1090	156	12	%	%	NOUN
eurjchem-1090	156	13	rsd	rsd	NOUN
eurjchem-1090	156	14	%	%	NOUN
eurjchem-1090	156	15	x±sd	x±sd	PROPN
eurjchem-1090	157	1	accuracy	accuracy	NOUN
eurjchem-1090	157	2	%	%	NOUN
eurjchem-1090	157	3	rsd	rsd	NOUN
eurjchem-1090	157	4	%	%	NOUN
eurjchem-1090	157	5	moexipril	moexipril	NOUN
eurjchem-1090	157	6	15	15	NUM
eurjchem-1090	157	7	14.56±1.41	14.56±1.41	NUM
eurjchem-1090	157	8	97.1	97.1	NUM
eurjchem-1090	157	9	9.68	9.68	NUM
eurjchem-1090	157	10	14.78±2.14	14.78±2.14	NUM
eurjchem-1090	157	11	98.5	98.5	NUM
eurjchem-1090	157	12	14.48	14.48	NUM
eurjchem-1090	157	13	50	50	NUM
eurjchem-1090	157	14	51.23±0.57	51.23±0.57	NUM
eurjchem-1090	157	15	102.5	102.5	NUM
eurjchem-1090	157	16	1.11	1.11	NUM
eurjchem-1090	157	17	48.89±1.87	48.89±1.87	NUM
eurjchem-1090	157	18	97.8	97.8	NUM
eurjchem-1090	157	19	3.82	3.82	NUM
eurjchem-1090	157	20	100	100	NUM
eurjchem-1090	157	21	98.63±1.37	98.63±1.37	NUM
eurjchem-1090	157	22	98.6	98.6	NUM
eurjchem-1090	157	23	1.39	1.39	NUM
eurjchem-1090	157	24	98.32±0.25	98.32±0.25	NUM
eurjchem-1090	157	25	98.3	98.3	NUM
eurjchem-1090	157	26	0.25	0.25	NUM
eurjchem-1090	157	27	moexiprilat	moexiprilat	NOUN
eurjchem-1090	157	28	5	5	NUM
eurjchem-1090	157	29	4.870±0.41	4.870±0.41	NUM
eurjchem-1090	157	30	97.4	97.4	NUM
eurjchem-1090	157	31	8.42	8.42	NUM
eurjchem-1090	157	32	4.840±0.23	4.840±0.23	NUM
eurjchem-1090	157	33	96.8	96.8	NUM
eurjchem-1090	157	34	4.75	4.75	NUM
eurjchem-1090	157	35	30	30	NUM
eurjchem-1090	157	36	29.47±1.25	29.47±1.25	NUM
eurjchem-1090	157	37	98.2	98.2	NUM
eurjchem-1090	157	38	4.24	4.24	NUM
eurjchem-1090	157	39	31.26±0.54	31.26±0.54	NUM
eurjchem-1090	157	40	104.2	104.2	NUM
eurjchem-1090	157	41	1.73	1.73	NUM
eurjchem-1090	157	42	100	100	NUM
eurjchem-1090	157	43	99.54±0.64	99.54±0.64	NUM
eurjchem-1090	157	44	99.5	99.5	NUM
eurjchem-1090	157	45	0.64	0.64	NUM
eurjchem-1090	157	46	99.78±2.54	99.78±2.54	NUM
eurjchem-1090	157	47	99.8	99.8	NUM
eurjchem-1090	157	48	2.55	2.55	NUM
eurjchem-1090	157	49	table	table	NOUN
eurjchem-1090	157	50	3	3	NUM
eurjchem-1090	157	51	.	.	PUNCT
eurjchem-1090	158	1	stability	stability	NOUN
eurjchem-1090	158	2	data	datum	NOUN
eurjchem-1090	158	3	of	of	ADP
eurjchem-1090	158	4	moexipril	moexipril	NOUN
eurjchem-1090	158	5	and	and	CCONJ
eurjchem-1090	158	6	moexiprilat	moexiprilat	NOUN
eurjchem-1090	158	7	in	in	ADP
eurjchem-1090	158	8	human	human	ADJ
eurjchem-1090	158	9	plasma	plasma	NOUN
eurjchem-1090	158	10	at	at	ADP
eurjchem-1090	158	11	various	various	ADJ
eurjchem-1090	158	12	conditions	condition	NOUN
eurjchem-1090	158	13	(	(	PUNCT
eurjchem-1090	158	14	n	n	NOUN
eurjchem-1090	158	15	=	=	SYM
eurjchem-1090	158	16	3	3	NUM
eurjchem-1090	158	17	)	)	PUNCT
eurjchem-1090	158	18	.	.	PUNCT
eurjchem-1090	159	1	analyte	analyte	NOUN
eurjchem-1090	159	2	c	c	PROPN
eurjchem-1090	159	3	(	(	PUNCT
eurjchem-1090	159	4	ng	ng	PROPN
eurjchem-1090	159	5	/	/	SYM
eurjchem-1090	159	6	ml	ml	NOUN
eurjchem-1090	159	7	)	)	PUNCT
eurjchem-1090	159	8	bench	bench	VERB
eurjchem-1090	159	9	top	top	NOUN
eurjchem-1090	159	10	(	(	PUNCT
eurjchem-1090	159	11	8	8	NUM
eurjchem-1090	159	12	h	h	NOUN
eurjchem-1090	159	13	)	)	PUNCT
eurjchem-1090	159	14	three	three	NUM
eurjchem-1090	159	15	freeze‐thaw	freeze‐thaw	NOUN
eurjchem-1090	159	16	moexipril	moexipril	NOUN
eurjchem-1090	159	17	15	15	NUM
eurjchem-1090	159	18	x±sd	x±sd	PROPN
eurjchem-1090	159	19	14.98±0.43	14.98±0.43	NUM
eurjchem-1090	159	20	14.21±3.14	14.21±3.14	NUM
eurjchem-1090	159	21	accuracy	accuracy	NOUN
eurjchem-1090	159	22	%	%	NOUN
eurjchem-1090	160	1	99.87	99.87	NUM
eurjchem-1090	160	2	94.73	94.73	NUM
eurjchem-1090	160	3	50	50	NUM
eurjchem-1090	160	4	x±sd	x±sd	SYM
eurjchem-1090	160	5	50.56±0.48	50.56±0.48	NUM
eurjchem-1090	160	6	48.87±2.87	48.87±2.87	NUM
eurjchem-1090	160	7	accuracy	accuracy	NOUN
eurjchem-1090	160	8	%	%	NOUN
eurjchem-1090	160	9	101.12	101.12	NUM
eurjchem-1090	160	10	97.74	97.74	NUM
eurjchem-1090	160	11	100	100	NUM
eurjchem-1090	160	12	x±sd	x±sd	ADP
eurjchem-1090	160	13	100.69±1.24	100.69±1.24	NUM
eurjchem-1090	160	14	101.24±3.04	101.24±3.04	NUM
eurjchem-1090	160	15	accuracy	accuracy	NOUN
eurjchem-1090	160	16	%	%	NOUN
eurjchem-1090	160	17	100.69	100.69	NUM
eurjchem-1090	160	18	101.24	101.24	NUM
eurjchem-1090	160	19	moexiprilat	moexiprilat	NOUN
eurjchem-1090	160	20	5	5	NUM
eurjchem-1090	160	21	x±sd	x±sd	NOUN
eurjchem-1090	160	22	5.08±1.12	5.08±1.12	NUM
eurjchem-1090	160	23	5.19±2.47	5.19±2.47	NUM
eurjchem-1090	160	24	accuracy	accuracy	NOUN
eurjchem-1090	160	25	%	%	NOUN
eurjchem-1090	160	26	101.60	101.60	NUM
eurjchem-1090	160	27	103.80	103.80	NUM
eurjchem-1090	160	28	30	30	NUM
eurjchem-1090	160	29	x±sd	x±sd	SYM
eurjchem-1090	160	30	30.87±0.76	30.87±0.76	PROPN
eurjchem-1090	161	1	31.65±2.41	31.65±2.41	NUM
eurjchem-1090	161	2	accuracy	accuracy	NOUN
eurjchem-1090	161	3	%	%	NOUN
eurjchem-1090	161	4	102.90	102.90	NUM
eurjchem-1090	161	5	105.50	105.50	NUM
eurjchem-1090	161	6	100	100	NUM
eurjchem-1090	161	7	x±sd	x±sd	ADP
eurjchem-1090	161	8	99.78±1.42	99.78±1.42	NUM
eurjchem-1090	161	9	98.78±0.58	98.78±0.58	NUM
eurjchem-1090	161	10	accuracy	accuracy	NOUN
eurjchem-1090	161	11	%	%	NOUN
eurjchem-1090	161	12	99.78	99.78	NUM
eurjchem-1090	161	13	98.78	98.78	NUM
eurjchem-1090	161	14	(	(	PUNCT
eurjchem-1090	161	15	a	a	NOUN
eurjchem-1090	161	16	)	)	PUNCT
eurjchem-1090	161	17	(	(	PUNCT
eurjchem-1090	161	18	b	b	X
eurjchem-1090	161	19	)	)	PUNCT
eurjchem-1090	161	20	(	(	PUNCT
eurjchem-1090	161	21	c	c	X
eurjchem-1090	161	22	)	)	PUNCT
eurjchem-1090	161	23	figure	figure	NOUN
eurjchem-1090	161	24	3	3	NUM
eurjchem-1090	161	25	.	.	PUNCT
eurjchem-1090	162	1	blank	blank	ADJ
eurjchem-1090	162	2	human	human	ADJ
eurjchem-1090	162	3	plasma	plasma	NOUN
eurjchem-1090	162	4	showing	show	VERB
eurjchem-1090	162	5	no	no	DET
eurjchem-1090	162	6	interference	interference	NOUN
eurjchem-1090	162	7	,	,	PUNCT
eurjchem-1090	162	8	a	a	DET
eurjchem-1090	162	9	)	)	PUNCT
eurjchem-1090	162	10	moexipril	moexipril	NOUN
eurjchem-1090	162	11	,	,	PUNCT
eurjchem-1090	162	12	(	(	PUNCT
eurjchem-1090	162	13	b	b	NOUN
eurjchem-1090	162	14	)	)	PUNCT
eurjchem-1090	162	15	moexiprilat	moexiprilat	NOUN
eurjchem-1090	162	16	,	,	PUNCT
eurjchem-1090	162	17	and	and	CCONJ
eurjchem-1090	162	18	(	(	PUNCT
eurjchem-1090	162	19	c	c	X
eurjchem-1090	162	20	)	)	PUNCT
eurjchem-1090	162	21	benazepril	benazepril	NOUN
eurjchem-1090	162	22	.	.	PUNCT
eurjchem-1090	163	1	3.2.6.1	3.2.6.1	X
eurjchem-1090	163	2	.	.	PUNCT
eurjchem-1090	163	3	short	short	ADJ
eurjchem-1090	163	4	term	term	NOUN
eurjchem-1090	163	5	stability	stability	NOUN
eurjchem-1090	163	6	bench	bench	VERB
eurjchem-1090	163	7	top	top	ADJ
eurjchem-1090	163	8	stability	stability	NOUN
eurjchem-1090	163	9	was	be	AUX
eurjchem-1090	163	10	checked	check	VERB
eurjchem-1090	163	11	for	for	ADP
eurjchem-1090	163	12	each	each	DET
eurjchem-1090	163	13	analyte	analyte	NOUN
eurjchem-1090	163	14	by	by	ADP
eurjchem-1090	163	15	leaving	leave	VERB
eurjchem-1090	163	16	the	the	DET
eurjchem-1090	163	17	spiked	spiked	ADJ
eurjchem-1090	163	18	human	human	ADJ
eurjchem-1090	163	19	plasma	plasma	NOUN
eurjchem-1090	163	20	for	for	ADP
eurjchem-1090	163	21	8	8	NUM
eurjchem-1090	163	22	hours	hour	NOUN
eurjchem-1090	163	23	on	on	ADP
eurjchem-1090	163	24	bench‐top	bench‐top	NOUN
eurjchem-1090	163	25	.	.	PUNCT
eurjchem-1090	164	1	the	the	DET
eurjchem-1090	164	2	concentration	concentration	NOUN
eurjchem-1090	164	3	of	of	ADP
eurjchem-1090	164	4	the	the	DET
eurjchem-1090	164	5	analytes	analyte	NOUN
eurjchem-1090	164	6	never	never	ADV
eurjchem-1090	164	7	falls	fall	VERB
eurjchem-1090	164	8	outside	outside	ADP
eurjchem-1090	164	9	the	the	DET
eurjchem-1090	164	10	accepted	accept	VERB
eurjchem-1090	164	11	range	range	NOUN
eurjchem-1090	164	12	as	as	SCONJ
eurjchem-1090	164	13	seen	see	VERB
eurjchem-1090	164	14	in	in	ADP
eurjchem-1090	164	15	table	table	NOUN
eurjchem-1090	164	16	3	3	NUM
eurjchem-1090	164	17	.	.	PUNCT
eurjchem-1090	165	1	(	(	PUNCT
eurjchem-1090	165	2	a	a	X
eurjchem-1090	165	3	)	)	PUNCT
eurjchem-1090	165	4	(	(	PUNCT
eurjchem-1090	165	5	b	b	X
eurjchem-1090	165	6	)	)	PUNCT
eurjchem-1090	165	7	(	(	PUNCT
eurjchem-1090	165	8	c	c	X
eurjchem-1090	165	9	)	)	PUNCT
eurjchem-1090	165	10	figure	figure	NOUN
eurjchem-1090	165	11	4	4	NUM
eurjchem-1090	165	12	.	.	PUNCT
eurjchem-1090	166	1	mrm	mrm	PROPN
eurjchem-1090	166	2	chromatograms	chromatogram	NOUN
eurjchem-1090	166	3	of	of	ADP
eurjchem-1090	166	4	moexipril	moexipril	NOUN
eurjchem-1090	166	5	(	(	PUNCT
eurjchem-1090	166	6	a	a	NOUN
eurjchem-1090	166	7	)	)	PUNCT
eurjchem-1090	166	8	,	,	PUNCT
eurjchem-1090	166	9	moexiprilat	moexiprilat	NOUN
eurjchem-1090	166	10	(	(	PUNCT
eurjchem-1090	166	11	b	b	NOUN
eurjchem-1090	166	12	)	)	PUNCT
eurjchem-1090	166	13	,	,	PUNCT
eurjchem-1090	166	14	and	and	CCONJ
eurjchem-1090	166	15	benazepril	benazepril	ADJ
eurjchem-1090	166	16	(	(	PUNCT
eurjchem-1090	166	17	c	c	NOUN
eurjchem-1090	166	18	)	)	PUNCT
eurjchem-1090	166	19	.	.	PUNCT
eurjchem-1090	167	1	3.2.6.2	3.2.6.2	X
eurjchem-1090	167	2	.	.	PUNCT
eurjchem-1090	167	3	freeze	freeze	NOUN
eurjchem-1090	167	4	and	and	CCONJ
eurjchem-1090	167	5	thaw	thaw	NOUN
eurjchem-1090	167	6	stability	stability	NOUN
eurjchem-1090	167	7	the	the	DET
eurjchem-1090	167	8	stability	stability	NOUN
eurjchem-1090	167	9	of	of	ADP
eurjchem-1090	167	10	the	the	DET
eurjchem-1090	167	11	analytes	analyte	NOUN
eurjchem-1090	167	12	in	in	ADP
eurjchem-1090	167	13	human	human	ADJ
eurjchem-1090	167	14	plasma	plasma	NOUN
eurjchem-1090	167	15	was	be	AUX
eurjchem-1090	167	16	investigated	investigate	VERB
eurjchem-1090	167	17	under	under	ADP
eurjchem-1090	167	18	the	the	DET
eurjchem-1090	167	19	conditions	condition	NOUN
eurjchem-1090	167	20	recommended	recommend	VERB
eurjchem-1090	167	21	by	by	ADP
eurjchem-1090	167	22	the	the	DET
eurjchem-1090	167	23	fda	fda	PROPN
eurjchem-1090	168	1	[	[	X
eurjchem-1090	168	2	12	12	NUM
eurjchem-1090	168	3	]	]	PUNCT
eurjchem-1090	168	4	.	.	PUNCT
eurjchem-1090	169	1	so	so	ADV
eurjchem-1090	169	2	,	,	PUNCT
eurjchem-1090	169	3	freeze‐thaw	freeze‐thaw	ADJ
eurjchem-1090	169	4	stability	stability	NOUN
eurjchem-1090	169	5	was	be	AUX
eurjchem-1090	169	6	assessed	assess	VERB
eurjchem-1090	169	7	with	with	ADP
eurjchem-1090	169	8	three	three	NUM
eurjchem-1090	169	9	sets	set	NOUN
eurjchem-1090	169	10	of	of	ADP
eurjchem-1090	169	11	stability	stability	NOUN
eurjchem-1090	169	12	control	control	NOUN
eurjchem-1090	169	13	samples	sample	NOUN
eurjchem-1090	169	14	after	after	ADP
eurjchem-1090	169	15	three	three	NUM
eurjchem-1090	169	16	freeze‐thaw	freeze‐thaw	NOUN
eurjchem-1090	169	17	cycles	cycle	NOUN
eurjchem-1090	169	18	and	and	CCONJ
eurjchem-1090	169	19	during	during	ADP
eurjchem-1090	169	20	storage	storage	NOUN
eurjchem-1090	169	21	at	at	ADP
eurjchem-1090	169	22	‐80	‐80	NOUN
eurjchem-1090	169	23	°	°	ADP
eurjchem-1090	169	24	c	c	NOUN
eurjchem-1090	169	25	up	up	ADP
eurjchem-1090	169	26	to	to	PART
eurjchem-1090	169	27	30	30	NUM
eurjchem-1090	169	28	days	day	NOUN
eurjchem-1090	169	29	(	(	PUNCT
eurjchem-1090	169	30	table	table	NOUN
eurjchem-1090	169	31	3	3	NUM
eurjchem-1090	169	32	)	)	PUNCT
eurjchem-1090	169	33	.	.	PUNCT
eurjchem-1090	170	1	elaziz	elaziz	PROPN
eurjchem-1090	170	2	et	et	PROPN
eurjchem-1090	170	3	al	al	PROPN
eurjchem-1090	170	4	.	.	PUNCT
eurjchem-1090	170	5	/	/	SYM
eurjchem-1090	170	6	european	european	PROPN
eurjchem-1090	170	7	journal	journal	PROPN
eurjchem-1090	170	8	of	of	ADP
eurjchem-1090	170	9	chemistry	chemistry	NOUN
eurjchem-1090	170	10	5	5	NUM
eurjchem-1090	170	11	(	(	PUNCT
eurjchem-1090	170	12	4	4	NUM
eurjchem-1090	170	13	)	)	PUNCT
eurjchem-1090	170	14	(	(	PUNCT
eurjchem-1090	170	15	2014	2014	NUM
eurjchem-1090	170	16	)	)	PUNCT
eurjchem-1090	170	17	662‐667	662‐667	NUM
eurjchem-1090	170	18	667	667	NUM
eurjchem-1090	170	19	table	table	NOUN
eurjchem-1090	170	20	4	4	NUM
eurjchem-1090	170	21	.	.	PUNCT
eurjchem-1090	171	1	statistical	statistical	ADJ
eurjchem-1090	171	2	comparison	comparison	NOUN
eurjchem-1090	171	3	for	for	ADP
eurjchem-1090	171	4	the	the	DET
eurjchem-1090	171	5	results	result	NOUN
eurjchem-1090	171	6	obtained	obtain	VERB
eurjchem-1090	171	7	by	by	ADP
eurjchem-1090	171	8	the	the	DET
eurjchem-1090	171	9	proposed	propose	VERB
eurjchem-1090	171	10	method	method	NOUN
eurjchem-1090	171	11	and	and	CCONJ
eurjchem-1090	171	12	the	the	DET
eurjchem-1090	171	13	reported	report	VERB
eurjchem-1090	171	14	method	method	NOUN
eurjchem-1090	171	15	[	[	X
eurjchem-1090	171	16	4	4	NUM
eurjchem-1090	171	17	]	]	PUNCT
eurjchem-1090	171	18	for	for	ADP
eurjchem-1090	171	19	the	the	DET
eurjchem-1090	171	20	analysis	analysis	NOUN
eurjchem-1090	171	21	of	of	ADP
eurjchem-1090	171	22	moexipril	moexipril	NOUN
eurjchem-1090	171	23	in	in	ADP
eurjchem-1090	171	24	bulk	bulk	ADJ
eurjchem-1090	171	25	powder	powder	NOUN
eurjchem-1090	171	26	.	.	PUNCT
eurjchem-1090	172	1	method	method	NOUN
eurjchem-1090	172	2	drug	drug	NOUN
eurjchem-1090	172	3	mean	mean	PROPN
eurjchem-1090	172	4	s.d	s.d	PROPN
eurjchem-1090	172	5	.	.	PROPN
eurjchem-1090	172	6	rsd%	rsd%	PROPN
eurjchem-1090	172	7	n	n	CCONJ
eurjchem-1090	172	8	variance	variance	NOUN
eurjchem-1090	172	9	student	student	NOUN
eurjchem-1090	172	10	's	's	PART
eurjchem-1090	172	11	t	t	PROPN
eurjchem-1090	172	12	test	test	NOUN
eurjchem-1090	172	13	(	(	PUNCT
eurjchem-1090	172	14	2.23	2.23	NUM
eurjchem-1090	172	15	)	)	PUNCT
eurjchem-1090	172	16	a	a	DET
eurjchem-1090	172	17	f	f	PROPN
eurjchem-1090	172	18	test	test	NOUN
eurjchem-1090	172	19	(	(	PUNCT
eurjchem-1090	172	20	5.05	5.05	NUM
eurjchem-1090	172	21	)	)	PUNCT
eurjchem-1090	172	22	a	a	DET
eurjchem-1090	172	23	lc	lc	PROPN
eurjchem-1090	172	24	/	/	SYM
eurjchem-1090	172	25	ms	ms	PROPN
eurjchem-1090	172	26	mox	mox	PROPN
eurjchem-1090	172	27	99.32	99.32	NUM
eurjchem-1090	172	28	2.77	2.77	NUM
eurjchem-1090	172	29	2.788	2.788	NUM
eurjchem-1090	172	30	6	6	NUM
eurjchem-1090	172	31	7.672	7.672	NUM
eurjchem-1090	172	32	0.258	0.258	NUM
eurjchem-1090	172	33	1.681	1.681	NUM
eurjchem-1090	172	34	reported	report	VERB
eurjchem-1090	172	35	method	method	NOUN
eurjchem-1090	172	36	[	[	X
eurjchem-1090	172	37	1	1	NUM
eurjchem-1090	172	38	]	]	SYM
eurjchem-1090	172	39	b	b	X
eurjchem-1090	172	40	mox	mox	NOUN
eurjchem-1090	172	41	99.24	99.24	NUM
eurjchem-1090	172	42	2.12	2.12	NUM
eurjchem-1090	172	43	2.136	2.136	NUM
eurjchem-1090	172	44	6	6	NUM
eurjchem-1090	172	45	4.562	4.562	NUM
eurjchem-1090	172	46	a	a	DET
eurjchem-1090	172	47	the	the	DET
eurjchem-1090	172	48	values	value	NOUN
eurjchem-1090	172	49	in	in	ADP
eurjchem-1090	172	50	parenthesis	parenthesis	NOUN
eurjchem-1090	172	51	are	be	AUX
eurjchem-1090	172	52	the	the	DET
eurjchem-1090	172	53	corresponding	corresponding	ADJ
eurjchem-1090	172	54	theoretical	theoretical	ADJ
eurjchem-1090	172	55	values	value	NOUN
eurjchem-1090	172	56	of	of	ADP
eurjchem-1090	172	57	t	t	PROPN
eurjchem-1090	172	58	and	and	CCONJ
eurjchem-1090	172	59	f	f	PROPN
eurjchem-1090	172	60	at	at	ADP
eurjchem-1090	172	61	p	p	NOUN
eurjchem-1090	172	62	=	=	NOUN
eurjchem-1090	172	63	0.05	0.05	NUM
eurjchem-1090	172	64	.	.	PUNCT
eurjchem-1090	173	1	b	b	NOUN
eurjchem-1090	173	2	separation	separation	NOUN
eurjchem-1090	173	3	was	be	AUX
eurjchem-1090	173	4	achieved	achieve	VERB
eurjchem-1090	173	5	on	on	ADP
eurjchem-1090	173	6	luna	luna	PROPN
eurjchem-1090	173	7	c18	c18	PROPN
eurjchem-1090	173	8	column	column	NOUN
eurjchem-1090	173	9	(	(	PUNCT
eurjchem-1090	173	10	250×4.6	250×4.6	NOUN
eurjchem-1090	173	11	mm	mm	PROPN
eurjchem-1090	173	12	i.d	i.d	PROPN
eurjchem-1090	173	13	.	.	PROPN
eurjchem-1090	173	14	,	,	PUNCT
eurjchem-1090	173	15	5	5	NUM
eurjchem-1090	173	16	um	um	INTJ
eurjchem-1090	173	17	,	,	PUNCT
eurjchem-1090	173	18	acetonitrile‐20	acetonitrile‐20	PROPN
eurjchem-1090	173	19	mm	mm	NUM
eurjchem-1090	173	20	phosphate	phosphate	NOUN
eurjchem-1090	173	21	buffer	buffer	NOUN
eurjchem-1090	173	22	(	(	PUNCT
eurjchem-1090	173	23	ph	ph	NOUN
eurjchem-1090	173	24	=	=	SYM
eurjchem-1090	173	25	4.0	4.0	NUM
eurjchem-1090	173	26	)	)	PUNCT
eurjchem-1090	173	27	(	(	PUNCT
eurjchem-1090	173	28	50:50	50:50	NUM
eurjchem-1090	173	29	,	,	PUNCT
eurjchem-1090	173	30	v	v	NOUN
eurjchem-1090	173	31	:	:	PUNCT
eurjchem-1090	173	32	v	v	NOUN
eurjchem-1090	173	33	)	)	PUNCT
eurjchem-1090	173	34	at	at	ADP
eurjchem-1090	173	35	a	a	DET
eurjchem-1090	173	36	flow	flow	NOUN
eurjchem-1090	173	37	rate	rate	NOUN
eurjchem-1090	173	38	of	of	ADP
eurjchem-1090	173	39	1	1	NUM
eurjchem-1090	173	40	ml	ml	NOUN
eurjchem-1090	173	41	/	/	SYM
eurjchem-1090	173	42	min	min	NOUN
eurjchem-1090	173	43	,	,	PUNCT
eurjchem-1090	173	44	and	and	CCONJ
eurjchem-1090	173	45	uv	uv	NOUN
eurjchem-1090	173	46	detection	detection	NOUN
eurjchem-1090	173	47	at	at	ADP
eurjchem-1090	173	48	212	212	NUM
eurjchem-1090	173	49	nm	nm	NOUN
eurjchem-1090	173	50	.	.	PUNCT
eurjchem-1090	174	1	(	(	PUNCT
eurjchem-1090	174	2	a	a	X
eurjchem-1090	174	3	)	)	PUNCT
eurjchem-1090	174	4	(	(	PUNCT
eurjchem-1090	174	5	b	b	X
eurjchem-1090	174	6	)	)	PUNCT
eurjchem-1090	174	7	(	(	PUNCT
eurjchem-1090	174	8	c	c	X
eurjchem-1090	174	9	)	)	PUNCT
eurjchem-1090	174	10	figure	figure	NOUN
eurjchem-1090	174	11	5	5	NUM
eurjchem-1090	174	12	.	.	PUNCT
eurjchem-1090	175	1	mrm	mrm	PROPN
eurjchem-1090	175	2	chromatograms	chromatogram	NOUN
eurjchem-1090	175	3	of	of	ADP
eurjchem-1090	175	4	moexipril	moexipril	NOUN
eurjchem-1090	175	5	(	(	PUNCT
eurjchem-1090	175	6	a	a	NOUN
eurjchem-1090	175	7	)	)	PUNCT
eurjchem-1090	175	8	,	,	PUNCT
eurjchem-1090	175	9	moexiprilat	moexiprilat	NOUN
eurjchem-1090	175	10	(	(	PUNCT
eurjchem-1090	175	11	b	b	NOUN
eurjchem-1090	175	12	)	)	PUNCT
eurjchem-1090	175	13	,	,	PUNCT
eurjchem-1090	175	14	and	and	CCONJ
eurjchem-1090	175	15	benazepril	benazepril	ADJ
eurjchem-1090	175	16	(	(	PUNCT
eurjchem-1090	175	17	c	c	NOUN
eurjchem-1090	175	18	)	)	PUNCT
eurjchem-1090	175	19	in	in	ADP
eurjchem-1090	175	20	spiked	spiked	ADJ
eurjchem-1090	175	21	human	human	ADJ
eurjchem-1090	175	22	plasma	plasma	NOUN
eurjchem-1090	175	23	.	.	PUNCT
eurjchem-1090	176	1	3.2.6.3	3.2.6.3	X
eurjchem-1090	176	2	.	.	PUNCT
eurjchem-1090	176	3	stock	stock	NOUN
eurjchem-1090	176	4	solution	solution	NOUN
eurjchem-1090	176	5	stability	stability	NOUN
eurjchem-1090	176	6	the	the	DET
eurjchem-1090	176	7	stability	stability	NOUN
eurjchem-1090	176	8	of	of	ADP
eurjchem-1090	176	9	the	the	DET
eurjchem-1090	176	10	mox	mox	NOUN
eurjchem-1090	176	11	,	,	PUNCT
eurjchem-1090	176	12	moxt	moxt	NOUN
eurjchem-1090	176	13	,	,	PUNCT
eurjchem-1090	176	14	and	and	CCONJ
eurjchem-1090	176	15	i.s	i.s	PROPN
eurjchem-1090	176	16	.	.	PROPN
eurjchem-1090	177	1	stock	stock	NOUN
eurjchem-1090	177	2	solutions	solution	NOUN
eurjchem-1090	177	3	was	be	AUX
eurjchem-1090	177	4	performed	perform	VERB
eurjchem-1090	177	5	by	by	ADP
eurjchem-1090	177	6	comparison	comparison	NOUN
eurjchem-1090	177	7	of	of	ADP
eurjchem-1090	177	8	results	result	NOUN
eurjchem-1090	177	9	from	from	ADP
eurjchem-1090	177	10	a	a	DET
eurjchem-1090	177	11	solution	solution	NOUN
eurjchem-1090	177	12	kept	keep	VERB
eurjchem-1090	177	13	for	for	ADP
eurjchem-1090	177	14	about	about	ADV
eurjchem-1090	177	15	60	60	NUM
eurjchem-1090	177	16	days	day	NOUN
eurjchem-1090	177	17	at	at	ADP
eurjchem-1090	177	18	4	4	NUM
eurjchem-1090	177	19	°	°	NOUN
eurjchem-1090	177	20	c	c	NOUN
eurjchem-1090	177	21	and	and	CCONJ
eurjchem-1090	177	22	from	from	ADP
eurjchem-1090	177	23	a	a	DET
eurjchem-1090	177	24	solution	solution	NOUN
eurjchem-1090	177	25	that	that	PRON
eurjchem-1090	177	26	was	be	AUX
eurjchem-1090	177	27	extempora‐	extempora‐	PROPN
eurjchem-1090	177	28	neously	neously	ADV
eurjchem-1090	177	29	prepared	prepare	VERB
eurjchem-1090	177	30	.	.	PUNCT
eurjchem-1090	178	1	for	for	ADP
eurjchem-1090	178	2	this	this	DET
eurjchem-1090	178	3	purpose	purpose	NOUN
eurjchem-1090	178	4	,	,	PUNCT
eurjchem-1090	178	5	three	three	NUM
eurjchem-1090	178	6	replicates	replicate	NOUN
eurjchem-1090	178	7	of	of	ADP
eurjchem-1090	178	8	each	each	DET
eurjchem-1090	178	9	analyte	analyte	NOUN
eurjchem-1090	178	10	were	be	AUX
eurjchem-1090	178	11	prepared	prepare	VERB
eurjchem-1090	178	12	from	from	ADP
eurjchem-1090	178	13	each	each	DET
eurjchem-1090	178	14	stock	stock	NOUN
eurjchem-1090	178	15	solution	solution	NOUN
eurjchem-1090	178	16	and	and	CCONJ
eurjchem-1090	178	17	injected	inject	VERB
eurjchem-1090	178	18	in	in	ADP
eurjchem-1090	178	19	the	the	DET
eurjchem-1090	178	20	lc‐ms	lc‐ms	NOUN
eurjchem-1090	178	21	/	/	SYM
eurjchem-1090	178	22	ms	ms	NOUN
eurjchem-1090	178	23	system	system	NOUN
eurjchem-1090	178	24	.	.	PUNCT
eurjchem-1090	179	1	the	the	DET
eurjchem-1090	179	2	same	same	ADJ
eurjchem-1090	179	3	test	test	NOUN
eurjchem-1090	179	4	was	be	AUX
eurjchem-1090	179	5	performed	perform	VERB
eurjchem-1090	179	6	with	with	ADP
eurjchem-1090	179	7	the	the	DET
eurjchem-1090	179	8	stock	stock	NOUN
eurjchem-1090	179	9	solutions	solution	NOUN
eurjchem-1090	179	10	of	of	ADP
eurjchem-1090	179	11	i.s	i.s	PROPN
eurjchem-1090	179	12	.	.	PROPN
eurjchem-1090	179	13	results	result	NOUN
eurjchem-1090	179	14	were	be	AUX
eurjchem-1090	179	15	compared	compare	VERB
eurjchem-1090	179	16	to	to	ADP
eurjchem-1090	179	17	freshly	freshly	ADV
eurjchem-1090	179	18	prepared	prepare	VERB
eurjchem-1090	179	19	solutions	solution	NOUN
eurjchem-1090	179	20	at	at	ADP
eurjchem-1090	179	21	corresponding	corresponding	ADJ
eurjchem-1090	179	22	concentration	concentration	NOUN
eurjchem-1090	179	23	as	as	SCONJ
eurjchem-1090	179	24	shown	show	VERB
eurjchem-1090	179	25	in	in	ADP
eurjchem-1090	179	26	table	table	NOUN
eurjchem-1090	179	27	3	3	NUM
eurjchem-1090	179	28	.	.	NOUN
eurjchem-1090	179	29	4	4	NUM
eurjchem-1090	179	30	.	.	X
eurjchem-1090	180	1	statistical	statistical	ADJ
eurjchem-1090	180	2	analysis	analysis	NOUN
eurjchem-1090	180	3	results	result	NOUN
eurjchem-1090	180	4	obtained	obtain	VERB
eurjchem-1090	180	5	by	by	ADP
eurjchem-1090	180	6	the	the	DET
eurjchem-1090	180	7	proposed	propose	VERB
eurjchem-1090	180	8	method	method	NOUN
eurjchem-1090	180	9	for	for	ADP
eurjchem-1090	180	10	the	the	DET
eurjchem-1090	180	11	deter‐	deter‐	NOUN
eurjchem-1090	180	12	mination	mination	NOUN
eurjchem-1090	180	13	of	of	ADP
eurjchem-1090	180	14	pure	pure	ADJ
eurjchem-1090	180	15	samples	sample	NOUN
eurjchem-1090	180	16	of	of	ADP
eurjchem-1090	180	17	mox	mox	NOUN
eurjchem-1090	180	18	and	and	CCONJ
eurjchem-1090	180	19	moxt	moxt	NOUN
eurjchem-1090	180	20	are	be	AUX
eurjchem-1090	180	21	statistically	statistically	ADV
eurjchem-1090	180	22	compared	compare	VERB
eurjchem-1090	180	23	to	to	ADP
eurjchem-1090	180	24	those	those	PRON
eurjchem-1090	180	25	obtained	obtain	VERB
eurjchem-1090	180	26	by	by	ADP
eurjchem-1090	180	27	the	the	DET
eurjchem-1090	180	28	reported	report	VERB
eurjchem-1090	180	29	methods4	methods4	PROPN
eurjchem-1090	180	30	.	.	PUNCT
eurjchem-1090	181	1	the	the	DET
eurjchem-1090	181	2	calculated	calculate	VERB
eurjchem-1090	181	3	t	t	PROPN
eurjchem-1090	181	4	and	and	CCONJ
eurjchem-1090	181	5	f	f	PROPN
eurjchem-1090	181	6	values	value	NOUN
eurjchem-1090	181	7	were	be	AUX
eurjchem-1090	181	8	found	find	VERB
eurjchem-1090	181	9	to	to	PART
eurjchem-1090	181	10	be	be	AUX
eurjchem-1090	181	11	less	less	ADJ
eurjchem-1090	181	12	than	than	ADP
eurjchem-1090	181	13	their	their	PRON
eurjchem-1090	181	14	corresponding	correspond	VERB
eurjchem-1090	181	15	theoretical	theoretical	ADJ
eurjchem-1090	181	16	ones	one	NOUN
eurjchem-1090	181	17	confirming	confirm	VERB
eurjchem-1090	181	18	good	good	ADJ
eurjchem-1090	181	19	accuracy	accuracy	NOUN
eurjchem-1090	181	20	and	and	CCONJ
eurjchem-1090	181	21	excellent	excellent	ADJ
eurjchem-1090	181	22	precision	precision	NOUN
eurjchem-1090	181	23	(	(	PUNCT
eurjchem-1090	181	24	table	table	NOUN
eurjchem-1090	181	25	4	4	NUM
eurjchem-1090	181	26	)	)	PUNCT
eurjchem-1090	181	27	.	.	PUNCT
eurjchem-1090	182	1	5	5	X
eurjchem-1090	182	2	.	.	X
eurjchem-1090	182	3	conclusions	conclusion	NOUN
eurjchem-1090	182	4	in	in	ADP
eurjchem-1090	182	5	the	the	DET
eurjchem-1090	182	6	present	present	ADJ
eurjchem-1090	182	7	study	study	NOUN
eurjchem-1090	182	8	,	,	PUNCT
eurjchem-1090	182	9	both	both	DET
eurjchem-1090	182	10	mox	mox	NOUN
eurjchem-1090	182	11	and	and	CCONJ
eurjchem-1090	182	12	its	its	PRON
eurjchem-1090	182	13	active	active	ADJ
eurjchem-1090	182	14	metabolite	metabolite	NOUN
eurjchem-1090	182	15	moxt	moxt	NOUN
eurjchem-1090	182	16	were	be	AUX
eurjchem-1090	182	17	determined	determine	VERB
eurjchem-1090	182	18	in	in	ADP
eurjchem-1090	182	19	spiked	spiked	ADJ
eurjchem-1090	182	20	human	human	ADJ
eurjchem-1090	182	21	plasma	plasma	NOUN
eurjchem-1090	182	22	by	by	ADP
eurjchem-1090	182	23	lc‐	lc‐	ADJ
eurjchem-1090	182	24	tandem	tandem	NOUN
eurjchem-1090	182	25	mass	mass	PROPN
eurjchem-1090	182	26	spectrometry	spectrometry	NOUN
eurjchem-1090	182	27	method	method	NOUN
eurjchem-1090	182	28	using	use	VERB
eurjchem-1090	182	29	one	one	NUM
eurjchem-1090	182	30	is	be	AUX
eurjchem-1090	182	31	.	.	PUNCT
eurjchem-1090	183	1	the	the	DET
eurjchem-1090	183	2	method	method	NOUN
eurjchem-1090	183	3	showed	show	VERB
eurjchem-1090	183	4	satisfactory	satisfactory	ADJ
eurjchem-1090	183	5	precision	precision	NOUN
eurjchem-1090	183	6	and	and	CCONJ
eurjchem-1090	183	7	accuracy	accuracy	NOUN
eurjchem-1090	183	8	results	result	NOUN
eurjchem-1090	183	9	.	.	PUNCT
eurjchem-1090	184	1	the	the	DET
eurjchem-1090	184	2	run	run	ADJ
eurjchem-1090	184	3	time	time	NOUN
eurjchem-1090	184	4	of	of	ADP
eurjchem-1090	184	5	the	the	DET
eurjchem-1090	184	6	developed	develop	VERB
eurjchem-1090	184	7	method	method	NOUN
eurjchem-1090	184	8	is	be	AUX
eurjchem-1090	184	9	too	too	ADV
eurjchem-1090	184	10	short	short	ADJ
eurjchem-1090	184	11	,	,	PUNCT
eurjchem-1090	184	12	so	so	SCONJ
eurjchem-1090	184	13	it	it	PRON
eurjchem-1090	184	14	can	can	AUX
eurjchem-1090	184	15	be	be	AUX
eurjchem-1090	184	16	used	use	VERB
eurjchem-1090	184	17	in	in	ADP
eurjchem-1090	184	18	bioequivalence	bioequivalence	NOUN
eurjchem-1090	184	19	studies	study	NOUN
eurjchem-1090	184	20	to	to	PART
eurjchem-1090	184	21	test	test	VERB
eurjchem-1090	184	22	maximum	maximum	ADJ
eurjchem-1090	184	23	number	number	NOUN
eurjchem-1090	184	24	of	of	ADP
eurjchem-1090	184	25	samples	sample	NOUN
eurjchem-1090	184	26	in	in	ADP
eurjchem-1090	184	27	a	a	DET
eurjchem-1090	184	28	short	short	ADJ
eurjchem-1090	184	29	time	time	NOUN
eurjchem-1090	184	30	.	.	PUNCT
eurjchem-1090	185	1	acknowledgements	acknowledgement	NOUN
eurjchem-1090	185	2	the	the	DET
eurjchem-1090	185	3	authors	author	NOUN
eurjchem-1090	185	4	are	be	AUX
eurjchem-1090	185	5	grateful	grateful	ADJ
eurjchem-1090	185	6	to	to	ADP
eurjchem-1090	185	7	dr	dr	PROPN
eurjchem-1090	185	8	.	.	PROPN
eurjchem-1090	185	9	ahmed	ahmed	PROPN
eurjchem-1090	185	10	hassan	hassan	PROPN
eurjchem-1090	185	11	,	,	PUNCT
eurjchem-1090	185	12	head	head	NOUN
eurjchem-1090	185	13	of	of	ADP
eurjchem-1090	185	14	genuine	genuine	ADJ
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eurjchem-1090	185	16	centre	centre	NOUN
eurjchem-1090	185	17	(	(	PUNCT
eurjchem-1090	185	18	grc	grc	PROPN
eurjchem-1090	185	19	)	)	PUNCT
eurjchem-1090	185	20	,	,	PUNCT
eurjchem-1090	185	21	cairo	cairo	PROPN
eurjchem-1090	185	22	,	,	PUNCT
eurjchem-1090	185	23	egypt	egypt	PROPN
eurjchem-1090	185	24	.	.	PUNCT
eurjchem-1090	186	1	the	the	DET
eurjchem-1090	186	2	authors	author	NOUN
eurjchem-1090	186	3	gratefully	gratefully	ADV
eurjchem-1090	186	4	acknowledge	acknowledge	VERB
eurjchem-1090	186	5	grc	grc	NOUN
eurjchem-1090	186	6	laboratories	laboratory	NOUN
eurjchem-1090	186	7	for	for	ADP
eurjchem-1090	186	8	their	their	PRON
eurjchem-1090	186	9	great	great	ADJ
eurjchem-1090	186	10	help	help	NOUN
eurjchem-1090	186	11	to	to	PART
eurjchem-1090	186	12	accomplish	accomplish	VERB
eurjchem-1090	186	13	this	this	DET
eurjchem-1090	186	14	work	work	NOUN
eurjchem-1090	186	15	.	.	PUNCT
eurjchem-1090	187	1	references	reference	NOUN
eurjchem-1090	187	2	[	[	X
eurjchem-1090	187	3	1	1	NUM
eurjchem-1090	187	4	]	]	PUNCT
eurjchem-1090	187	5	.	.	PUNCT
eurjchem-1090	188	1	moffat	moffat	PROPN
eurjchem-1090	188	2	,	,	PUNCT
eurjchem-1090	188	3	a.	a.	PROPN
eurjchem-1090	188	4	c.	c.	PROPN
eurjchem-1090	188	5	;	;	PUNCT
eurjchem-1090	188	6	osselton	osselton	PROPN
eurjchem-1090	188	7	,	,	PUNCT
eurjchem-1090	188	8	m.	m.	PROPN
eurjchem-1090	188	9	d.	d.	PROPN
eurjchem-1090	188	10	;	;	PUNCT
eurjchem-1090	188	11	widdop	widdop	PROPN
eurjchem-1090	188	12	,	,	PUNCT
eurjchem-1090	188	13	b.	b.	PROPN
eurjchem-1090	188	14	clarke	clarke	PROPN
eurjchem-1090	188	15	’s	’s	PART
eurjchem-1090	188	16	analysis	analysis	NOUN
eurjchem-1090	188	17	of	of	ADP
eurjchem-1090	188	18	drugs	drug	NOUN
eurjchem-1090	188	19	and	and	CCONJ
eurjchem-1090	188	20	poisons	poison	NOUN
eurjchem-1090	188	21	,	,	PUNCT
eurjchem-1090	188	22	pharmaceutical	pharmaceutical	NOUN
eurjchem-1090	188	23	press	press	NOUN
eurjchem-1090	188	24	,	,	PUNCT
eurjchem-1090	188	25	london	london	PROPN
eurjchem-1090	188	26	,	,	PUNCT
eurjchem-1090	188	27	uk	uk	PROPN
eurjchem-1090	188	28	,	,	PUNCT
eurjchem-1090	188	29	2005	2005	NUM
eurjchem-1090	188	30	.	.	PUNCT
eurjchem-1090	189	1	[	[	X
eurjchem-1090	189	2	2	2	NUM
eurjchem-1090	189	3	]	]	PUNCT
eurjchem-1090	189	4	.	.	PUNCT
eurjchem-1090	190	1	brogden	brogden	PROPN
eurjchem-1090	190	2	,	,	PUNCT
eurjchem-1090	190	3	r.	r.	PROPN
eurjchem-1090	190	4	n.	n.	PROPN
eurjchem-1090	190	5	;	;	PUNCT
eurjchem-1090	190	6	wiseman	wiseman	PROPN
eurjchem-1090	190	7	,	,	PUNCT
eurjchem-1090	190	8	l.	l.	PROPN
eurjchem-1090	190	9	r.	r.	PROPN
eurjchem-1090	190	10	drugs	drugs	PROPN
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eurjchem-1090	190	12	,	,	PUNCT
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eurjchem-1090	190	14	,	,	PUNCT
eurjchem-1090	190	15	845‐860	845‐860	PROPN
eurjchem-1090	190	16	.	.	PUNCT
eurjchem-1090	191	1	[	[	X
eurjchem-1090	191	2	3	3	NUM
eurjchem-1090	191	3	]	]	PUNCT
eurjchem-1090	191	4	.	.	PUNCT
eurjchem-1090	191	5	chrysant	chrysant	PROPN
eurjchem-1090	191	6	,	,	PUNCT
eurjchem-1090	191	7	s.	s.	PROPN
eurjchem-1090	191	8	g.	g.	PROPN
eurjchem-1090	191	9	;	;	PUNCT
eurjchem-1090	191	10	chrysant	chrysant	NOUN
eurjchem-1090	191	11	,	,	PUNCT
eurjchem-1090	191	12	g.	g.	PROPN
eurjchem-1090	191	13	s.	s.	PROPN
eurjchem-1090	191	14	j.	j.	PROPN
eurjchem-1090	191	15	clin	clin	PROPN
eurjchem-1090	191	16	.	.	PUNCT
eurjchem-1090	192	1	pharmacol	pharmacol	PROPN
eurjchem-1090	192	2	.	.	PUNCT
eurjchem-1090	193	1	2004	2004	NUM
eurjchem-1090	193	2	,	,	PUNCT
eurjchem-1090	193	3	44	44	NUM
eurjchem-1090	193	4	,	,	PUNCT
eurjchem-1090	193	5	827‐836	827‐836	NUM
eurjchem-1090	193	6	.	.	PUNCT
eurjchem-1090	194	1	[	[	X
eurjchem-1090	194	2	4	4	NUM
eurjchem-1090	194	3	]	]	PUNCT
eurjchem-1090	194	4	.	.	PUNCT
eurjchem-1090	194	5	stanisz	stanisz	PROPN
eurjchem-1090	194	6	,	,	PUNCT
eurjchem-1090	194	7	b.	b.	PROPN
eurjchem-1090	194	8	;	;	PUNCT
eurjchem-1090	194	9	regulska	regulska	PROPN
eurjchem-1090	194	10	,	,	PUNCT
eurjchem-1090	194	11	k.	k.	PROPN
eurjchem-1090	194	12	;	;	PUNCT
eurjchem-1090	194	13	ratajczak	ratajczak	PROPN
eurjchem-1090	194	14	,	,	PUNCT
eurjchem-1090	194	15	t.	t.	PROPN
eurjchem-1090	194	16	acta	acta	PROPN
eurjchem-1090	194	17	pol	pol	PROPN
eurjchem-1090	194	18	.	.	PUNCT
eurjchem-1090	195	1	pharm	pharm	PROPN
eurjchem-1090	195	2	.	.	PUNCT
eurjchem-1090	196	1	drug	drug	NOUN
eurjchem-1090	196	2	res	re	NOUN
eurjchem-1090	196	3	.	.	PROPN
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eurjchem-1090	196	5	,	,	PUNCT
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eurjchem-1090	196	7	,	,	PUNCT
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eurjchem-1090	196	9	.	.	PUNCT
eurjchem-1090	197	1	[	[	X
eurjchem-1090	197	2	5	5	NUM
eurjchem-1090	197	3	]	]	PUNCT
eurjchem-1090	197	4	.	.	PUNCT
eurjchem-1090	198	1	latha	latha	PROPN
eurjchem-1090	198	2	,	,	PUNCT
eurjchem-1090	198	3	y.	y.	PROPN
eurjchem-1090	198	4	b.	b.	PROPN
eurjchem-1090	198	5	;	;	PUNCT
eurjchem-1090	198	6	sankar	sankar	PROPN
eurjchem-1090	198	7	,	,	PUNCT
eurjchem-1090	198	8	d.	d.	PROPN
eurjchem-1090	198	9	g.	g.	PROPN
eurjchem-1090	198	10	int	int	PROPN
eurjchem-1090	198	11	.	.	PUNCT
eurjchem-1090	199	1	j.	j.	PROPN
eurjchem-1090	199	2	univ	univ	PROPN
eurjchem-1090	199	3	.	.	PUNCT
eurjchem-1090	200	1	pharm	pharm	PROPN
eurjchem-1090	200	2	.	.	PUNCT
eurjchem-1090	201	1	life	life	PROPN
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eurjchem-1090	201	3	.	.	PROPN
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eurjchem-1090	201	5	,	,	PUNCT
eurjchem-1090	201	6	1	1	NUM
eurjchem-1090	201	7	,	,	PUNCT
eurjchem-1090	201	8	156‐165	156‐165	NUM
eurjchem-1090	201	9	.	.	PUNCT
eurjchem-1090	202	1	[	[	X
eurjchem-1090	202	2	6	6	NUM
eurjchem-1090	202	3	]	]	PUNCT
eurjchem-1090	202	4	.	.	PUNCT
eurjchem-1090	203	1	elshanawane	elshanawane	ADJ
eurjchem-1090	203	2	,	,	PUNCT
eurjchem-1090	203	3	a.	a.	NOUN
eurjchem-1090	203	4	a.	a.	PROPN
eurjchem-1090	203	5	;	;	PUNCT
eurjchem-1090	203	6	mostafa	mostafa	PROPN
eurjchem-1090	203	7	,	,	PUNCT
eurjchem-1090	203	8	s.	s.	PROPN
eurjchem-1090	203	9	m.	m.	PROPN
eurjchem-1090	203	10	;	;	PUNCT
eurjchem-1090	203	11	elgawish	elgawish	PROPN
eurjchem-1090	203	12	,	,	PUNCT
eurjchem-1090	203	13	m.	m.	NOUN
eurjchem-1090	203	14	s.	s.	PROPN
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eurjchem-1090	203	17	,	,	PUNCT
eurjchem-1090	203	18	67	67	NUM
eurjchem-1090	203	19	,	,	PUNCT
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eurjchem-1090	203	21	.	.	PUNCT
eurjchem-1090	204	1	[	[	X
eurjchem-1090	204	2	7	7	NUM
eurjchem-1090	204	3	]	]	PUNCT
eurjchem-1090	204	4	.	.	PUNCT
eurjchem-1090	205	1	pandey	pandey	PROPN
eurjchem-1090	205	2	,	,	PUNCT
eurjchem-1090	205	3	r.	r.	PROPN
eurjchem-1090	205	4	;	;	PUNCT
eurjchem-1090	205	5	patil	patil	PROPN
eurjchem-1090	205	6	,	,	PUNCT
eurjchem-1090	205	7	p.	p.	PROPN
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eurjchem-1090	205	9	;	;	PUNCT
eurjchem-1090	205	10	bari	bari	NOUN
eurjchem-1090	205	11	,	,	PUNCT
eurjchem-1090	205	12	s.	s.	PROPN
eurjchem-1090	205	13	b.	b.	PROPN
eurjchem-1090	205	14	;	;	PUNCT
eurjchem-1090	205	15	dhumal	dhumal	PROPN
eurjchem-1090	205	16	,	,	PUNCT
eurjchem-1090	205	17	d.	d.	PROPN
eurjchem-1090	205	18	m.	m.	PROPN
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eurjchem-1090	205	22	.	.	PUNCT
eurjchem-1090	206	1	pharm	pharm	PROPN
eurjchem-1090	206	2	.	.	PUNCT
eurjchem-1090	207	1	res	re	NOUN
eurjchem-1090	207	2	.	.	PROPN
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eurjchem-1090	207	4	,	,	PUNCT
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eurjchem-1090	207	6	,	,	PUNCT
eurjchem-1090	207	7	342‐347	342‐347	PROPN
eurjchem-1090	207	8	.	.	PUNCT
eurjchem-1090	208	1	[	[	X
eurjchem-1090	208	2	8	8	NUM
eurjchem-1090	208	3	]	]	PUNCT
eurjchem-1090	208	4	.	.	PUNCT
eurjchem-1090	209	1	abd	abd	PROPN
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eurjchem-1090	209	4	,	,	PUNCT
eurjchem-1090	209	5	m.	m.	NOUN
eurjchem-1090	209	6	;	;	PUNCT
eurjchem-1090	209	7	el	el	PROPN
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eurjchem-1090	209	9	,	,	PUNCT
eurjchem-1090	209	10	a.	a.	PROPN
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eurjchem-1090	209	12	;	;	PUNCT
eurjchem-1090	209	13	hegazy	hegazy	ADV
eurjchem-1090	209	14	,	,	PUNCT
eurjchem-1090	209	15	m.	m.	NOUN
eurjchem-1090	209	16	;	;	PUNCT
eurjchem-1090	209	17	shokry	shokry	PROPN
eurjchem-1090	209	18	,	,	PUNCT
eurjchem-1090	209	19	e.	e.	PROPN
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eurjchem-1090	209	21	j.	j.	PROPN
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eurjchem-1090	209	23	.	.	PUNCT
eurjchem-1090	210	1	sci	sci	PROPN
eurjchem-1090	210	2	.	.	PUNCT
eurjchem-1090	210	3	res	res	PROPN
eurjchem-1090	210	4	.	.	PUNCT
eurjchem-1090	210	5	2010	2010	NUM
eurjchem-1090	210	6	,	,	PUNCT
eurjchem-1090	210	7	6	6	NUM
eurjchem-1090	210	8	,	,	PUNCT
eurjchem-1090	210	9	918‐926	918‐926	NUM
eurjchem-1090	210	10	.	.	PUNCT
eurjchem-1090	211	1	[	[	X
eurjchem-1090	211	2	9	9	NUM
eurjchem-1090	211	3	]	]	PUNCT
eurjchem-1090	211	4	.	.	PUNCT
eurjchem-1090	212	1	hammes	hammes	PROPN
eurjchem-1090	212	2	,	,	PUNCT
eurjchem-1090	212	3	w.	w.	PROPN
eurjchem-1090	212	4	;	;	PUNCT
eurjchem-1090	212	5	hammes	hammes	PROPN
eurjchem-1090	212	6	,	,	PUNCT
eurjchem-1090	212	7	b.	b.	PROPN
eurjchem-1090	212	8	;	;	PUNCT
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eurjchem-1090	212	10	,	,	PUNCT
eurjchem-1090	212	11	u.	u.	PROPN
eurjchem-1090	212	12	;	;	PUNCT
eurjchem-1090	212	13	paar	paar	PROPN
eurjchem-1090	212	14	,	,	PUNCT
eurjchem-1090	212	15	f.	f.	PROPN
eurjchem-1090	212	16	;	;	PUNCT
eurjchem-1090	212	17	bökens	bökens	PROPN
eurjchem-1090	212	18	,	,	PUNCT
eurjchem-1090	212	19	h.	h.	PROPN
eurjchem-1090	212	20	j.	j.	PROPN
eurjchem-1090	212	21	chromatogr	chromatogr	PROPN
eurjchem-1090	212	22	.	.	PUNCT
eurjchem-1090	213	1	b	b	X
eurjchem-1090	213	2	:	:	PUNCT
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eurjchem-1090	213	4	.	.	PUNCT
eurjchem-1090	214	1	technol	technol	PROPN
eurjchem-1090	214	2	.	.	PROPN
eurjchem-1090	214	3	biomed	biome	VERB
eurjchem-1090	214	4	.	.	PUNCT
eurjchem-1090	215	1	life	life	PROPN
eurjchem-1090	215	2	sci	sci	PROPN
eurjchem-1090	215	3	.	.	PROPN
eurjchem-1090	215	4	1995	1995	NUM
eurjchem-1090	215	5	,	,	PUNCT
eurjchem-1090	215	6	670	670	NUM
eurjchem-1090	215	7	,	,	PUNCT
eurjchem-1090	215	8	81‐89	81‐89	PRON
eurjchem-1090	215	9	.	.	PUNCT
eurjchem-1090	216	1	[	[	X
eurjchem-1090	216	2	10	10	NUM
eurjchem-1090	216	3	]	]	PUNCT
eurjchem-1090	216	4	.	.	PUNCT
eurjchem-1090	217	1	koti	koti	PROPN
eurjchem-1090	217	2	,	,	PUNCT
eurjchem-1090	217	3	j.	j.	PROPN
eurjchem-1090	217	4	;	;	PUNCT
eurjchem-1090	217	5	hada	hada	PROPN
eurjchem-1090	217	6	,	,	PUNCT
eurjchem-1090	217	7	v.	v.	PROPN
eurjchem-1090	217	8	;	;	PUNCT
eurjchem-1090	217	9	petroianu	petroianu	NOUN
eurjchem-1090	217	10	,	,	PUNCT
eurjchem-1090	217	11	g.	g.	PROPN
eurjchem-1090	217	12	;	;	PUNCT
eurjchem-1090	217	13	hasan	hasan	PROPN
eurjchem-1090	217	14	,	,	PUNCT
eurjchem-1090	217	15	m.	m.	NOUN
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eurjchem-1090	217	17	;	;	PUNCT
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eurjchem-1090	217	19	,	,	PUNCT
eurjchem-1090	217	20	k.	k.	PROPN
eurjchem-1090	217	21	;	;	PUNCT
eurjchem-1090	217	22	szücs	szücs	PROPN
eurjchem-1090	217	23	,	,	PUNCT
eurjchem-1090	217	24	z.	z.	PROPN
eurjchem-1090	217	25	;	;	PUNCT
eurjchem-1090	217	26	kalasz	kalasz	PROPN
eurjchem-1090	217	27	,	,	PUNCT
eurjchem-1090	217	28	h.	h.	PROPN
eurjchem-1090	217	29	j.	j.	PROPN
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eurjchem-1090	217	31	.	.	PUNCT
eurjchem-1090	218	1	sci	sci	PROPN
eurjchem-1090	218	2	.	.	PROPN
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eurjchem-1090	218	4	,	,	PUNCT
eurjchem-1090	218	5	44	44	NUM
eurjchem-1090	218	6	,	,	PUNCT
eurjchem-1090	218	7	214‐218	214‐218	NOUN
eurjchem-1090	218	8	.	.	PUNCT
eurjchem-1090	219	1	[	[	X
eurjchem-1090	219	2	11	11	NUM
eurjchem-1090	219	3	]	]	PUNCT
eurjchem-1090	219	4	.	.	PUNCT
eurjchem-1090	219	5	karra	karra	NOUN
eurjchem-1090	219	6	,	,	PUNCT
eurjchem-1090	219	7	v.	v.	PROPN
eurjchem-1090	219	8	k.	k.	PROPN
eurjchem-1090	219	9	;	;	PUNCT
eurjchem-1090	219	10	mullangi	mullangi	PROPN
eurjchem-1090	219	11	,	,	PUNCT
eurjchem-1090	219	12	r.	r.	PROPN
eurjchem-1090	219	13	;	;	PUNCT
eurjchem-1090	219	14	pilli	pilli	PROPN
eurjchem-1090	219	15	,	,	PUNCT
eurjchem-1090	219	16	n.	n.	PROPN
eurjchem-1090	219	17	r.	r.	PROPN
eurjchem-1090	219	18	;	;	PUNCT
eurjchem-1090	219	19	inamadugu	inamadugu	PROPN
eurjchem-1090	219	20	,	,	PUNCT
eurjchem-1090	219	21	j.	j.	PROPN
eurjchem-1090	219	22	k.	k.	PROPN
eurjchem-1090	219	23	;	;	PUNCT
eurjchem-1090	219	24	ravi	ravi	PROPN
eurjchem-1090	219	25	,	,	PUNCT
eurjchem-1090	219	26	v.	v.	PROPN
eurjchem-1090	219	27	b.	b.	PROPN
eurjchem-1090	219	28	;	;	PUNCT
eurjchem-1090	219	29	seshagiri	seshagiri	ADV
eurjchem-1090	219	30	,	,	PUNCT
eurjchem-1090	219	31	j.	j.	PROPN
eurjchem-1090	219	32	v.	v.	PROPN
eurjchem-1090	219	33	biomed	biome	VERB
eurjchem-1090	219	34	.	.	PUNCT
eurjchem-1090	220	1	chromatogr	chromatogr	PROPN
eurjchem-1090	220	2	.	.	PUNCT
eurjchem-1090	221	1	2012	2012	NUM
eurjchem-1090	221	2	,	,	PUNCT
eurjchem-1090	221	3	26	26	NUM
eurjchem-1090	221	4	,	,	PUNCT
eurjchem-1090	221	5	1552‐1558	1552‐1558	NUM
eurjchem-1090	221	6	.	.	PUNCT
eurjchem-1090	222	1	[	[	X
eurjchem-1090	222	2	12	12	NUM
eurjchem-1090	222	3	]	]	PUNCT
eurjchem-1090	222	4	.	.	PUNCT
eurjchem-1090	223	1	guidance	guidance	NOUN
eurjchem-1090	223	2	for	for	ADP
eurjchem-1090	223	3	industry	industry	NOUN
eurjchem-1090	223	4	,	,	PUNCT
eurjchem-1090	223	5	bioanalytical	bioanalytical	ADJ
eurjchem-1090	223	6	method	method	NOUN
eurjchem-1090	223	7	validation	validation	NOUN
eurjchem-1090	223	8	,	,	PUNCT
eurjchem-1090	223	9	us	us	PROPN
eurjchem-1090	223	10	department	department	PROPN
eurjchem-1090	223	11	of	of	ADP
eurjchem-1090	223	12	health	health	PROPN
eurjchem-1090	223	13	and	and	CCONJ
eurjchem-1090	223	14	human	human	ADJ
eurjchem-1090	223	15	services	service	NOUN
eurjchem-1090	223	16	,	,	PUNCT
eurjchem-1090	223	17	food	food	NOUN
eurjchem-1090	223	18	and	and	CCONJ
eurjchem-1090	223	19	drug	drug	NOUN
eurjchem-1090	223	20	administration	administration	NOUN
eurjchem-1090	223	21	,	,	PUNCT
eurjchem-1090	223	22	center	center	NOUN
eurjchem-1090	223	23	for	for	ADP
eurjchem-1090	223	24	drug	drug	NOUN
eurjchem-1090	223	25	evaluation	evaluation	NOUN
eurjchem-1090	223	26	and	and	CCONJ
eurjchem-1090	223	27	research	research	NOUN
eurjchem-1090	223	28	(	(	PUNCT
eurjchem-1090	223	29	cder	cder	NOUN
eurjchem-1090	223	30	)	)	PUNCT
eurjchem-1090	223	31	center	center	NOUN
eurjchem-1090	223	32	for	for	ADP
eurjchem-1090	223	33	veterinary	veterinary	ADJ
eurjchem-1090	223	34	medicine	medicine	NOUN
eurjchem-1090	223	35	(	(	PUNCT
eurjchem-1090	223	36	cvm	cvm	PROPN
eurjchem-1090	223	37	)	)	PUNCT
eurjchem-1090	223	38	,	,	PUNCT
eurjchem-1090	223	39	usa	usa	PROPN
eurjchem-1090	223	40	,	,	PUNCT
eurjchem-1090	223	41	2001	2001	NUM
eurjchem-1090	223	42	.	.	PUNCT