id sid tid token lemma pos eurjchem-112 1 1 microsoft microsoft PROPN eurjchem-112 1 2 word word NOUN eurjchem-112 1 3 european_journal_of_chemistry_1_3_2010_232_235_112 european_journal_of_chemistry_1_3_2010_232_235_112 PROPN eurjchem-112 1 4 european european ADJ eurjchem-112 1 5     SPACE eurjchem-112 1 6 journal journal NOUN eurjchem-112 1 7     SPACE eurjchem-112 1 8 of of ADP eurjchem-112 1 9     SPACE eurjchem-112 1 10 chemistry chemistry NOUN eurjchem-112 1 11     SPACE eurjchem-112 1 12 1 1 NUM eurjchem-112 1 13     SPACE eurjchem-112 1 14 ( ( PUNCT eurjchem-112 1 15 3 3 NUM eurjchem-112 1 16 ) ) PUNCT eurjchem-112 1 17     SPACE eurjchem-112 1 18 ( ( PUNCT eurjchem-112 1 19 2010 2010 NUM eurjchem-112 1 20 ) ) PUNCT eurjchem-112 1 21     SPACE eurjchem-112 1 22 232‐235 232‐235 NUM eurjchem-112 1 23         SPACE eurjchem-112 1 24 european european ADJ eurjchem-112 1 25     SPACE eurjchem-112 1 26 journal journal NOUN eurjchem-112 1 27     SPACE eurjchem-112 1 28 of of ADP eurjchem-112 1 29     SPACE eurjchem-112 1 30 chemistry chemistry NOUN eurjchem-112 1 31     SPACE eurjchem-112 1 32 issn issn VERB eurjchem-112 1 33     SPACE eurjchem-112 1 34 2153‐2249 2153‐2249 NUM eurjchem-112 1 35     SPACE eurjchem-112 1 36 ( ( PUNCT eurjchem-112 1 37 print print NOUN eurjchem-112 1 38 ) ) PUNCT eurjchem-112 1 39     SPACE eurjchem-112 1 40 / / SYM eurjchem-112 1 41     SPACE eurjchem-112 1 42 issn issn VERB eurjchem-112 1 43     SPACE eurjchem-112 1 44 2153‐2257 2153‐2257 NUM eurjchem-112 1 45     SPACE eurjchem-112 1 46 ( ( PUNCT eurjchem-112 1 47 online online ADJ eurjchem-112 1 48 ) ) PUNCT eurjchem-112 1 49     SPACE eurjchem-112 1 50   NOUN eurjchem-112 1 51     SPACE eurjchem-112 1 52 2010 2010 NUM eurjchem-112 1 53     SPACE eurjchem-112 1 54 eurjchem eurjchem NOUN eurjchem-112 1 55     SPACE eurjchem-112 1 56 doi:10.5155 doi:10.5155 PROPN eurjchem-112 1 57 / / SYM eurjchem-112 1 58 eurjchem.1.3.232‐235.112 eurjchem.1.3.232‐235.112 PROPN eurjchem-112 1 59                 SPACE eurjchem-112 1 60 european european ADJ eurjchem-112 1 61     SPACE eurjchem-112 1 62 journal journal NOUN eurjchem-112 1 63     SPACE eurjchem-112 1 64 of of ADP eurjchem-112 1 65     SPACE eurjchem-112 1 66 chemistry chemistry NOUN eurjchem-112 1 67     SPACE eurjchem-112 1 68 journal journal NOUN eurjchem-112 1 69     SPACE eurjchem-112 1 70 homepage homepage NOUN eurjchem-112 1 71 : : PUNCT eurjchem-112 1 72     SPACE eurjchem-112 1 73 www.eurjchem.com www.eurjchem.com NOUN eurjchem-112 1 74                     SPACE eurjchem-112 1 75 dabco dabco NOUN eurjchem-112 1 76     SPACE eurjchem-112 1 77 as as ADP eurjchem-112 1 78     SPACE eurjchem-112 1 79 an an DET eurjchem-112 1 80     SPACE eurjchem-112 1 81 efficient efficient ADJ eurjchem-112 1 82     SPACE eurjchem-112 1 83 catalyst catalyst NOUN eurjchem-112 1 84     SPACE eurjchem-112 1 85 for for ADP eurjchem-112 1 86     SPACE eurjchem-112 1 87 the the DET eurjchem-112 1 88     SPACE eurjchem-112 1 89 synthesis synthesis NOUN eurjchem-112 1 90     SPACE eurjchem-112 1 91 of of ADP eurjchem-112 1 92     SPACE eurjchem-112 1 93 3‐cyano‐2(1h)‐pyridinones 3‐cyano‐2(1h)‐pyridinone NOUN eurjchem-112 1 94     SPACE eurjchem-112 1 95 and and CCONJ eurjchem-112 1 96     SPACE eurjchem-112 1 97 their their PRON eurjchem-112 1 98     SPACE eurjchem-112 1 99 2‐imino 2‐imino NOUN eurjchem-112 1 100     SPACE eurjchem-112 1 101 analogues analogue NOUN eurjchem-112 1 102     SPACE eurjchem-112 1 103 yahia yahia PROPN eurjchem-112 1 104     SPACE eurjchem-112 1 105 shirazi shirazi PROPN eurjchem-112 1 106     SPACE eurjchem-112 1 107 beheshtia beheshtia PROPN eurjchem-112 1 108 , , PUNCT eurjchem-112 1 109     SPACE eurjchem-112 1 110 maliheh maliheh PROPN eurjchem-112 1 111     SPACE eurjchem-112 1 112 khorshidi khorshidi NOUN eurjchem-112 1 113 , , PUNCT eurjchem-112 1 114     SPACE eurjchem-112 1 115 majid majid PROPN eurjchem-112 1 116     SPACE eurjchem-112 1 117 momahed momahe VERB eurjchem-112 1 118     SPACE eurjchem-112 1 119 heravi heravi NOUN eurjchem-112 1 120 * * PUNCT eurjchem-112 1 121     SPACE eurjchem-112 1 122 and and CCONJ eurjchem-112 1 123     SPACE eurjchem-112 1 124 bita bita PROPN eurjchem-112 1 125     SPACE eurjchem-112 1 126 baghernejad baghernejad PROPN eurjchem-112 1 127     SPACE eurjchem-112 1 128 department department NOUN eurjchem-112 1 129     SPACE eurjchem-112 1 130 of of ADP eurjchem-112 1 131     SPACE eurjchem-112 1 132 chemistry chemistry NOUN eurjchem-112 1 133 , , PUNCT eurjchem-112 1 134     SPACE eurjchem-112 1 135 school school NOUN eurjchem-112 1 136     SPACE eurjchem-112 1 137 of of ADP eurjchem-112 1 138     SPACE eurjchem-112 1 139 science science NOUN eurjchem-112 1 140 , , PUNCT eurjchem-112 1 141     SPACE eurjchem-112 1 142 azzahra azzahra PROPN eurjchem-112 1 143     SPACE eurjchem-112 1 144 university university NOUN eurjchem-112 1 145 , , PUNCT eurjchem-112 1 146     SPACE eurjchem-112 1 147 vanak vanak NOUN eurjchem-112 1 148 , , PUNCT eurjchem-112 1 149     SPACE eurjchem-112 1 150 tehran tehran PROPN eurjchem-112 1 151 , , PUNCT eurjchem-112 1 152     SPACE eurjchem-112 1 153 ir19569 ir19569 PROPN eurjchem-112 1 154 , , PUNCT eurjchem-112 1 155     SPACE eurjchem-112 1 156 iran iran PROPN eurjchem-112 1 157     SPACE eurjchem-112 1 158 * * PUNCT eurjchem-112 1 159 corresponding corresponding ADJ eurjchem-112 1 160     SPACE eurjchem-112 1 161 author author NOUN eurjchem-112 1 162     SPACE eurjchem-112 1 163 at at ADP eurjchem-112 1 164 : : PUNCT eurjchem-112 1 165     SPACE eurjchem-112 1 166 department department NOUN eurjchem-112 1 167     SPACE eurjchem-112 1 168 of of ADP eurjchem-112 1 169     SPACE eurjchem-112 1 170 chemistry chemistry NOUN eurjchem-112 1 171 , , PUNCT eurjchem-112 1 172     SPACE eurjchem-112 1 173 school school NOUN eurjchem-112 1 174     SPACE eurjchem-112 1 175 of of ADP eurjchem-112 1 176     SPACE eurjchem-112 1 177 science science NOUN eurjchem-112 1 178 , , PUNCT eurjchem-112 1 179     SPACE eurjchem-112 1 180 azzahra azzahra PROPN eurjchem-112 1 181     SPACE eurjchem-112 1 182 university university NOUN eurjchem-112 1 183 , , PUNCT eurjchem-112 1 184     SPACE eurjchem-112 1 185 vanak vanak NOUN eurjchem-112 1 186 , , PUNCT eurjchem-112 1 187     SPACE eurjchem-112 1 188 tehran tehran PROPN eurjchem-112 1 189 , , PUNCT eurjchem-112 1 190     SPACE eurjchem-112 1 191 ir19569 ir19569 PROPN eurjchem-112 1 192 , , PUNCT eurjchem-112 1 193     SPACE eurjchem-112 1 194 iran iran PROPN eurjchem-112 1 195 . . PUNCT eurjchem-112 1 196     SPACE eurjchem-112 2 1 tel tel PROPN eurjchem-112 2 2 . . PUNCT eurjchem-112 2 3 : : PUNCT eurjchem-112 2 4     SPACE eurjchem-112 2 5 +982188041344 +982188041344 NUM eurjchem-112 2 6 ; ; PUNCT eurjchem-112 2 7       SPACE eurjchem-112 2 8 fax fax NOUN eurjchem-112 2 9 : : PUNCT eurjchem-112 2 10     SPACE eurjchem-112 2 11 +982188047861 +982188047861 ADJ eurjchem-112 2 12 . . PUNCT eurjchem-112 2 13     SPACE eurjchem-112 2 14 e­mail e­mail NOUN eurjchem-112 2 15     SPACE eurjchem-112 2 16 address address NOUN eurjchem-112 2 17 : : PUNCT eurjchem-112 2 18     SPACE eurjchem-112 2 19 mmh1331@yahoo.com mmh1331@yahoo.com NOUN eurjchem-112 2 20     SPACE eurjchem-112 2 21 ( ( PUNCT eurjchem-112 2 22 m.m m.m PROPN eurjchem-112 2 23 . . PROPN eurjchem-112 2 24     SPACE eurjchem-112 2 25 heravi heravi NOUN eurjchem-112 2 26 ) ) PUNCT eurjchem-112 2 27 . . PUNCT eurjchem-112 2 28                                 SPACE eurjchem-112 2 29 communication communication NOUN eurjchem-112 2 30     SPACE eurjchem-112 2 31 information information NOUN eurjchem-112 2 32         SPACE eurjchem-112 2 33 abstract abstract ADJ eurjchem-112 2 34 received receive VERB eurjchem-112 2 35 : : PUNCT eurjchem-112 2 36     SPACE eurjchem-112 2 37 17 17 NUM eurjchem-112 2 38     SPACE eurjchem-112 2 39 may may AUX eurjchem-112 2 40     SPACE eurjchem-112 2 41 2010 2010 NUM eurjchem-112 2 42     SPACE eurjchem-112 2 43 received receive VERB eurjchem-112 2 44     SPACE eurjchem-112 2 45 in in ADP eurjchem-112 2 46     SPACE eurjchem-112 2 47 revised revise VERB eurjchem-112 2 48     SPACE eurjchem-112 2 49 form form NOUN eurjchem-112 2 50 : : PUNCT eurjchem-112 2 51     SPACE eurjchem-112 2 52 7 7 NUM eurjchem-112 2 53     SPACE eurjchem-112 2 54 june june PROPN eurjchem-112 2 55     SPACE eurjchem-112 2 56 2010 2010 NUM eurjchem-112 2 57     SPACE eurjchem-112 2 58 accepted accept VERB eurjchem-112 2 59 : : PUNCT eurjchem-112 2 60     SPACE eurjchem-112 2 61 8 8 NUM eurjchem-112 2 62     SPACE eurjchem-112 2 63 july july PROPN eurjchem-112 2 64     SPACE eurjchem-112 2 65 2010 2010 NUM eurjchem-112 2 66     SPACE eurjchem-112 2 67 online online NOUN eurjchem-112 2 68 : : PUNCT eurjchem-112 2 69     SPACE eurjchem-112 2 70 30 30 NUM eurjchem-112 2 71     SPACE eurjchem-112 2 72 september september PROPN eurjchem-112 2 73       SPACE eurjchem-112 2 74 2010 2010 NUM eurjchem-112 2 75     SPACE eurjchem-112 2 76 keywords keyword VERB eurjchem-112 2 77         SPACE eurjchem-112 2 78 3‐cyano‐2(1h)‐pyridinones 3‐cyano‐2(1h)‐pyridinone NOUN eurjchem-112 2 79     SPACE eurjchem-112 2 80 and and CCONJ eurjchem-112 2 81     SPACE eurjchem-112 2 82 their their PRON eurjchem-112 2 83     SPACE eurjchem-112 2 84 2‐imino 2‐imino NOUN eurjchem-112 2 85     SPACE eurjchem-112 2 86 analogues analogue NOUN eurjchem-112 2 87     SPACE eurjchem-112 2 88 have have AUX eurjchem-112 2 89     SPACE eurjchem-112 2 90 been be AUX eurjchem-112 2 91     SPACE eurjchem-112 2 92 synthesized synthesize VERB eurjchem-112 2 93     SPACE eurjchem-112 2 94 in in ADP eurjchem-112 2 95     SPACE eurjchem-112 2 96 good good ADJ eurjchem-112 2 97     SPACE eurjchem-112 2 98 yields yield NOUN eurjchem-112 2 99     SPACE eurjchem-112 2 100 via via ADP eurjchem-112 2 101     SPACE eurjchem-112 2 102 a a DET eurjchem-112 2 103     SPACE eurjchem-112 2 104 one‐pot one‐pot NOUN eurjchem-112 2 105     SPACE eurjchem-112 2 106 multi multi ADJ eurjchem-112 2 107 – – PUNCT eurjchem-112 2 108 component component NOUN eurjchem-112 2 109     SPACE eurjchem-112 2 110 reaction reaction NOUN eurjchem-112 2 111     SPACE eurjchem-112 2 112 of of ADP eurjchem-112 2 113     SPACE eurjchem-112 2 114 3,4‐dimethoxyacetophenone 3,4‐dimethoxyacetophenone NOUN eurjchem-112 2 115 , , PUNCT eurjchem-112 2 116     SPACE eurjchem-112 2 117 malononitrile malononitrile NOUN eurjchem-112 2 118     SPACE eurjchem-112 2 119 or or CCONJ eurjchem-112 2 120     SPACE eurjchem-112 2 121 ethylcyanoacetate ethylcyanoacetate VERB eurjchem-112 2 122 , , PUNCT eurjchem-112 2 123     SPACE eurjchem-112 2 124 ammonium ammonium NOUN eurjchem-112 2 125     SPACE eurjchem-112 2 126 acetate acetate NOUN eurjchem-112 2 127     SPACE eurjchem-112 2 128 and and CCONJ eurjchem-112 2 129     SPACE eurjchem-112 2 130 various various ADJ eurjchem-112 2 131     SPACE eurjchem-112 2 132 aldehydes aldehyde NOUN eurjchem-112 2 133     SPACE eurjchem-112 2 134 in in ADP eurjchem-112 2 135     SPACE eurjchem-112 2 136 the the DET eurjchem-112 2 137     SPACE eurjchem-112 2 138 presence presence NOUN eurjchem-112 2 139     SPACE eurjchem-112 2 140 of of ADP eurjchem-112 2 141       SPACE eurjchem-112 2 142 1,4‐diaza‐ 1,4‐diaza‐ PROPN eurjchem-112 2 143 bicyclo[2,2,2]octane bicyclo[2,2,2]octane NOUN eurjchem-112 2 144     SPACE eurjchem-112 2 145 ( ( PUNCT eurjchem-112 2 146 dabco dabco PROPN eurjchem-112 2 147 ) ) PUNCT eurjchem-112 2 148     SPACE eurjchem-112 2 149 in in ADP eurjchem-112 2 150     SPACE eurjchem-112 2 151 ethanol ethanol NOUN eurjchem-112 2 152 . . PUNCT eurjchem-112 2 153     SPACE eurjchem-112 3 1 dabco dabco PROPN eurjchem-112 3 2     SPACE eurjchem-112 3 3 has have AUX eurjchem-112 3 4     SPACE eurjchem-112 3 5 been be AUX eurjchem-112 3 6     SPACE eurjchem-112 3 7 widely widely ADV eurjchem-112 3 8     SPACE eurjchem-112 3 9 used use VERB eurjchem-112 3 10     SPACE eurjchem-112 3 11 as as ADP eurjchem-112 3 12     SPACE eurjchem-112 3 13 a a DET eurjchem-112 3 14     SPACE eurjchem-112 3 15 catalyst catalyst NOUN eurjchem-112 3 16     SPACE eurjchem-112 3 17 for for ADP eurjchem-112 3 18     SPACE eurjchem-112 3 19 the the DET eurjchem-112 3 20     SPACE eurjchem-112 3 21 organic organic ADJ eurjchem-112 3 22     SPACE eurjchem-112 3 23 reactions reaction NOUN eurjchem-112 3 24     SPACE eurjchem-112 3 25 and and CCONJ eurjchem-112 3 26     SPACE eurjchem-112 3 27 we we PRON eurjchem-112 3 28     SPACE eurjchem-112 3 29 selected select VERB eurjchem-112 3 30     SPACE eurjchem-112 3 31 it it PRON eurjchem-112 3 32     SPACE eurjchem-112 3 33 as as ADP eurjchem-112 3 34     SPACE eurjchem-112 3 35 an an DET eurjchem-112 3 36     SPACE eurjchem-112 3 37 efficient efficient ADJ eurjchem-112 3 38     SPACE eurjchem-112 3 39 catalyst catalyst NOUN eurjchem-112 3 40     SPACE eurjchem-112 3 41 to to PART eurjchem-112 3 42     SPACE eurjchem-112 3 43 synthesis synthesis NOUN eurjchem-112 3 44     SPACE eurjchem-112 3 45 of of ADP eurjchem-112 3 46     SPACE eurjchem-112 3 47 3‐cyano‐pyridines 3‐cyano‐pyridine NOUN eurjchem-112 3 48 . . PUNCT eurjchem-112 3 49     SPACE eurjchem-112 3 50 all all DET eurjchem-112 3 51     SPACE eurjchem-112 3 52 products product NOUN eurjchem-112 3 53     SPACE eurjchem-112 3 54 were be AUX eurjchem-112 3 55     SPACE eurjchem-112 3 56 characterized characterize VERB eurjchem-112 3 57     SPACE eurjchem-112 3 58 by by ADP eurjchem-112 3 59     SPACE eurjchem-112 3 60 melting melting NOUN eurjchem-112 3 61     SPACE eurjchem-112 3 62 point point NOUN eurjchem-112 3 63 , , PUNCT eurjchem-112 3 64     SPACE eurjchem-112 3 65 ir ir PROPN eurjchem-112 3 66 , , PUNCT eurjchem-112 3 67     SPACE eurjchem-112 3 68 1h 1h NUM eurjchem-112 3 69     SPACE eurjchem-112 3 70 nmr nmr NOUN eurjchem-112 3 71     SPACE eurjchem-112 3 72 and and CCONJ eurjchem-112 3 73     SPACE eurjchem-112 3 74 gc gc PROPN eurjchem-112 3 75 / / SYM eurjchem-112 3 76 ms ms NOUN eurjchem-112 3 77     SPACE eurjchem-112 3 78 studies study NOUN eurjchem-112 3 79 . . PUNCT eurjchem-112 3 80     SPACE eurjchem-112 4 1 1,4‐diaza‐bicyclo[2,2,2]octane 1,4‐diaza‐bicyclo[2,2,2]octane NUM eurjchem-112 4 2       SPACE eurjchem-112 4 3 cyano‐2(1h)‐pyridinones cyano‐2(1h)‐pyridinone NOUN eurjchem-112 4 4     SPACE eurjchem-112 4 5 cyano‐2(1h)‐iminopyridines cyano‐2(1h)‐iminopyridine NOUN eurjchem-112 4 6     SPACE eurjchem-112 4 7 3,4‐dimethoxyacetophenone 3,4‐dimethoxyacetophenone NUM eurjchem-112 4 8     SPACE eurjchem-112 4 9 dabco dabco NOUN eurjchem-112 4 10     SPACE eurjchem-112 4 11 catalyst catalyst NOUN eurjchem-112 4 12         SPACE eurjchem-112 4 13 1 1 NUM eurjchem-112 4 14 . . PUNCT eurjchem-112 4 15     SPACE eurjchem-112 4 16 introduction introduction NOUN eurjchem-112 4 17         SPACE eurjchem-112 4 18 heteroaromatic heteroaromatic ADJ eurjchem-112 4 19     SPACE eurjchem-112 4 20 rings ring NOUN eurjchem-112 4 21     SPACE eurjchem-112 4 22 containing contain VERB eurjchem-112 4 23     SPACE eurjchem-112 4 24 nitrogen nitrogen NOUN eurjchem-112 4 25     SPACE eurjchem-112 4 26 atoms atom NOUN eurjchem-112 4 27     SPACE eurjchem-112 4 28 often often ADV eurjchem-112 4 29     SPACE eurjchem-112 4 30 play play VERB eurjchem-112 4 31     SPACE eurjchem-112 4 32 important important ADJ eurjchem-112 4 33     SPACE eurjchem-112 4 34 roles role NOUN eurjchem-112 4 35     SPACE eurjchem-112 4 36 as as SCONJ eurjchem-112 4 37     SPACE eurjchem-112 4 38 the the DET eurjchem-112 4 39     SPACE eurjchem-112 4 40 heteroaromatics heteroaromatic NOUN eurjchem-112 4 41     SPACE eurjchem-112 4 42 incorporated incorporate VERB eurjchem-112 4 43     SPACE eurjchem-112 4 44 into into ADP eurjchem-112 4 45     SPACE eurjchem-112 4 46 the the DET eurjchem-112 4 47     SPACE eurjchem-112 4 48 structure structure NOUN eurjchem-112 4 49     SPACE eurjchem-112 4 50 of of ADP eurjchem-112 4 51     SPACE eurjchem-112 4 52 many many ADJ eurjchem-112 4 53     SPACE eurjchem-112 4 54 pharmaceuticals pharmaceutical NOUN eurjchem-112 4 55 . . PUNCT eurjchem-112 4 56     SPACE eurjchem-112 4 57 therefore therefore ADV eurjchem-112 4 58 , , PUNCT eurjchem-112 4 59     SPACE eurjchem-112 4 60 development development NOUN eurjchem-112 4 61     SPACE eurjchem-112 4 62 of of ADP eurjchem-112 4 63     SPACE eurjchem-112 4 64 efficient efficient ADJ eurjchem-112 4 65     SPACE eurjchem-112 4 66 procedures procedure NOUN eurjchem-112 4 67     SPACE eurjchem-112 4 68 towards towards ADP eurjchem-112 4 69     SPACE eurjchem-112 4 70 functionalized functionalize VERB eurjchem-112 4 71     SPACE eurjchem-112 4 72 pyridines pyridine NOUN eurjchem-112 4 73     SPACE eurjchem-112 4 74 is be AUX eurjchem-112 4 75     SPACE eurjchem-112 4 76 a a DET eurjchem-112 4 77     SPACE eurjchem-112 4 78 quite quite ADV eurjchem-112 4 79     SPACE eurjchem-112 4 80 attractive attractive ADJ eurjchem-112 4 81     SPACE eurjchem-112 4 82 target target NOUN eurjchem-112 4 83     SPACE eurjchem-112 4 84 for for ADP eurjchem-112 4 85     SPACE eurjchem-112 4 86 organic organic ADJ eurjchem-112 4 87     SPACE eurjchem-112 4 88 synthesis synthesis NOUN eurjchem-112 4 89 . . PUNCT eurjchem-112 4 90     SPACE eurjchem-112 5 1 3‐cyano‐pyridines 3‐cyano‐pyridine NOUN eurjchem-112 5 2     SPACE eurjchem-112 5 3 are be AUX eurjchem-112 5 4     SPACE eurjchem-112 5 5 of of ADP eurjchem-112 5 6     SPACE eurjchem-112 5 7 interest interest NOUN eurjchem-112 5 8     SPACE eurjchem-112 5 9 as as SCONJ eurjchem-112 5 10     SPACE eurjchem-112 5 11 they they PRON eurjchem-112 5 12     SPACE eurjchem-112 5 13 are be AUX eurjchem-112 5 14     SPACE eurjchem-112 5 15 used use VERB eurjchem-112 5 16     SPACE eurjchem-112 5 17 as as ADP eurjchem-112 5 18     SPACE eurjchem-112 5 19 intermediates intermediate NOUN eurjchem-112 5 20     SPACE eurjchem-112 5 21 for for ADP eurjchem-112 5 22     SPACE eurjchem-112 5 23 the the DET eurjchem-112 5 24     SPACE eurjchem-112 5 25 synthesis synthesis NOUN eurjchem-112 5 26     SPACE eurjchem-112 5 27 of of ADP eurjchem-112 5 28     SPACE eurjchem-112 5 29 variety variety NOUN eurjchem-112 5 30     SPACE eurjchem-112 5 31 of of ADP eurjchem-112 5 32     SPACE eurjchem-112 5 33 heterocyclic heterocyclic NOUN eurjchem-112 5 34     SPACE eurjchem-112 5 35 compounds compound VERB eurjchem-112 5 36     SPACE eurjchem-112 5 37 [ [ X eurjchem-112 5 38 2‐4 2‐4 NUM eurjchem-112 5 39 ] ] PUNCT eurjchem-112 5 40 . . PUNCT eurjchem-112 5 41     SPACE eurjchem-112 5 42 the the DET eurjchem-112 5 43     SPACE eurjchem-112 5 44 formation formation NOUN eurjchem-112 5 45     SPACE eurjchem-112 5 46 of of ADP eurjchem-112 5 47     SPACE eurjchem-112 5 48 2‐ 2‐ NUM eurjchem-112 5 49 oxo‐ oxo‐ NOUN eurjchem-112 5 50     SPACE eurjchem-112 5 51 and and CCONJ eurjchem-112 5 52     SPACE eurjchem-112 5 53 2‐iminopyridine 2‐iminopyridine NUM eurjchem-112 5 54     SPACE eurjchem-112 5 55 derivatives derivative NOUN eurjchem-112 5 56     SPACE eurjchem-112 5 57 were be AUX eurjchem-112 5 58     SPACE eurjchem-112 5 59 assumed assume VERB eurjchem-112 5 60     SPACE eurjchem-112 5 61 to to PART eurjchem-112 5 62     SPACE eurjchem-112 5 63 proceed proceed VERB eurjchem-112 5 64     SPACE eurjchem-112 5 65 via via ADP eurjchem-112 5 66     SPACE eurjchem-112 5 67 the the DET eurjchem-112 5 68     SPACE eurjchem-112 5 69 michael michael PROPN eurjchem-112 5 70     SPACE eurjchem-112 5 71 condensation condensation NOUN eurjchem-112 5 72     SPACE eurjchem-112 5 73 of of ADP eurjchem-112 5 74     SPACE eurjchem-112 5 75 ethyl ethyl NOUN eurjchem-112 5 76     SPACE eurjchem-112 5 77 cyanoacetate cyanoacetate NOUN eurjchem-112 5 78     SPACE eurjchem-112 5 79 or or CCONJ eurjchem-112 5 80     SPACE eurjchem-112 5 81 malononitrile malononitrile NOUN eurjchem-112 5 82     SPACE eurjchem-112 5 83 with with ADP eurjchem-112 5 84     SPACE eurjchem-112 5 85 α α NOUN eurjchem-112 5 86 , , PUNCT eurjchem-112 5 87     SPACE eurjchem-112 5 88 β‐unsaturated β‐unsaturated NUM eurjchem-112 5 89     SPACE eurjchem-112 5 90 ketone ketone NOUN eurjchem-112 5 91 , , PUNCT eurjchem-112 5 92     SPACE eurjchem-112 5 93 initially initially ADV eurjchem-112 5 94     SPACE eurjchem-112 5 95 formed form VERB eurjchem-112 5 96     SPACE eurjchem-112 5 97 from from ADP eurjchem-112 5 98     SPACE eurjchem-112 5 99 the the DET eurjchem-112 5 100     SPACE eurjchem-112 5 101 reaction reaction NOUN eurjchem-112 5 102     SPACE eurjchem-112 5 103 of of ADP eurjchem-112 5 104     SPACE eurjchem-112 5 105 the the DET eurjchem-112 5 106     SPACE eurjchem-112 5 107 aldehyde aldehyde NOUN eurjchem-112 5 108     SPACE eurjchem-112 5 109 with with ADP eurjchem-112 5 110     SPACE eurjchem-112 5 111 acetophenone acetophenone NOUN eurjchem-112 5 112     SPACE eurjchem-112 6 1 [ [ X eurjchem-112 6 2 5 5 NUM eurjchem-112 6 3 ] ] PUNCT eurjchem-112 6 4 . . PUNCT eurjchem-112 6 5     SPACE eurjchem-112 6 6 alternatively alternatively ADV eurjchem-112 6 7 , , PUNCT eurjchem-112 6 8     SPACE eurjchem-112 6 9 the the DET eurjchem-112 6 10     SPACE eurjchem-112 6 11 formation formation NOUN eurjchem-112 6 12     SPACE eurjchem-112 6 13 of of ADP eurjchem-112 6 14     SPACE eurjchem-112 6 15 2‐iminopyridines 2‐iminopyridine NOUN eurjchem-112 6 16     SPACE eurjchem-112 6 17 was be AUX eurjchem-112 6 18     SPACE eurjchem-112 6 19 explained explain VERB eurjchem-112 6 20     SPACE eurjchem-112 6 21 by by ADP eurjchem-112 6 22     SPACE eurjchem-112 6 23 the the DET eurjchem-112 6 24     SPACE eurjchem-112 6 25 initial initial ADJ eurjchem-112 6 26     SPACE eurjchem-112 6 27 formation formation NOUN eurjchem-112 6 28     SPACE eurjchem-112 6 29 of of ADP eurjchem-112 6 30     SPACE eurjchem-112 6 31 the the DET eurjchem-112 6 32     SPACE eurjchem-112 6 33 arylidene arylidene NOUN eurjchem-112 6 34     SPACE eurjchem-112 6 35 malononitrile malononitrile NOUN eurjchem-112 6 36     SPACE eurjchem-112 6 37 from from ADP eurjchem-112 6 38     SPACE eurjchem-112 6 39 the the DET eurjchem-112 6 40     SPACE eurjchem-112 6 41 aldehyde aldehyde NOUN eurjchem-112 6 42     SPACE eurjchem-112 6 43 and and CCONJ eurjchem-112 6 44     SPACE eurjchem-112 6 45 malononitrile malononitrile NOUN eurjchem-112 6 46     SPACE eurjchem-112 6 47 followed follow VERB eurjchem-112 6 48     SPACE eurjchem-112 6 49 by by ADP eurjchem-112 6 50     SPACE eurjchem-112 6 51 its its PRON eurjchem-112 6 52     SPACE eurjchem-112 6 53 subsequent subsequent ADJ eurjchem-112 6 54     SPACE eurjchem-112 6 55 reaction reaction NOUN eurjchem-112 6 56     SPACE eurjchem-112 6 57 with with ADP eurjchem-112 6 58     SPACE eurjchem-112 6 59 acetophenone acetophenone NOUN eurjchem-112 6 60     SPACE eurjchem-112 7 1 [ [ X eurjchem-112 7 2 5,6 5,6 NUM eurjchem-112 7 3 ] ] X eurjchem-112 7 4 . . PUNCT eurjchem-112 7 5     SPACE eurjchem-112 8 1 many many ADJ eurjchem-112 8 2     SPACE eurjchem-112 8 3 of of ADP eurjchem-112 8 4     SPACE eurjchem-112 8 5 the the DET eurjchem-112 8 6     SPACE eurjchem-112 8 7 standard standard ADJ eurjchem-112 8 8     SPACE eurjchem-112 8 9 procedures procedure NOUN eurjchem-112 8 10     SPACE eurjchem-112 8 11 require require NOUN eurjchem-112 8 12     SPACE eurjchem-112 8 13 either either ADV eurjchem-112 8 14     SPACE eurjchem-112 8 15 longer long ADJ eurjchem-112 8 16     SPACE eurjchem-112 8 17 reaction reaction NOUN eurjchem-112 8 18     SPACE eurjchem-112 8 19 times time NOUN eurjchem-112 8 20     SPACE eurjchem-112 8 21 or or CCONJ eurjchem-112 8 22     SPACE eurjchem-112 8 23 in in ADP eurjchem-112 8 24     SPACE eurjchem-112 8 25 some some DET eurjchem-112 8 26     SPACE eurjchem-112 8 27 cases case NOUN eurjchem-112 8 28 , , PUNCT eurjchem-112 8 29     SPACE eurjchem-112 8 30 lead lead NOUN eurjchem-112 8 31     SPACE eurjchem-112 8 32 to to ADP eurjchem-112 8 33     SPACE eurjchem-112 8 34 the the DET eurjchem-112 8 35     SPACE eurjchem-112 8 36 mixtures mixture NOUN eurjchem-112 8 37     SPACE eurjchem-112 8 38 of of ADP eurjchem-112 8 39     SPACE eurjchem-112 8 40 products product NOUN eurjchem-112 8 41     SPACE eurjchem-112 8 42 and and CCONJ eurjchem-112 8 43     SPACE eurjchem-112 8 44 resulted result VERB eurjchem-112 8 45     SPACE eurjchem-112 8 46 in in ADP eurjchem-112 8 47     SPACE eurjchem-112 8 48 low low ADJ eurjchem-112 8 49     SPACE eurjchem-112 8 50 yields yield NOUN eurjchem-112 8 51 . . PUNCT eurjchem-112 8 52     SPACE eurjchem-112 9 1 in in ADP eurjchem-112 9 2     SPACE eurjchem-112 9 3 view view NOUN eurjchem-112 9 4     SPACE eurjchem-112 9 5 of of ADP eurjchem-112 9 6     SPACE eurjchem-112 9 7 the the DET eurjchem-112 9 8     SPACE eurjchem-112 9 9 emerging emerge VERB eurjchem-112 9 10     SPACE eurjchem-112 9 11 importance importance NOUN eurjchem-112 9 12     SPACE eurjchem-112 9 13 of of ADP eurjchem-112 9 14     SPACE eurjchem-112 9 15 3‐cyano‐pyridines 3‐cyano‐pyridine NOUN eurjchem-112 9 16 , , PUNCT eurjchem-112 9 17     SPACE eurjchem-112 9 18 there there PRON eurjchem-112 9 19     SPACE eurjchem-112 9 20 still still ADV eurjchem-112 9 21     SPACE eurjchem-112 9 22 is be AUX eurjchem-112 9 23     SPACE eurjchem-112 9 24 a a DET eurjchem-112 9 25     SPACE eurjchem-112 9 26 need need NOUN eurjchem-112 9 27     SPACE eurjchem-112 9 28 to to PART eurjchem-112 9 29     SPACE eurjchem-112 9 30 introduce introduce VERB eurjchem-112 9 31     SPACE eurjchem-112 9 32 new new ADJ eurjchem-112 9 33     SPACE eurjchem-112 9 34 methods method NOUN eurjchem-112 9 35     SPACE eurjchem-112 9 36 for for ADP eurjchem-112 9 37     SPACE eurjchem-112 9 38 the the DET eurjchem-112 9 39     SPACE eurjchem-112 9 40 synthesis synthesis NOUN eurjchem-112 9 41     SPACE eurjchem-112 9 42 of of ADP eurjchem-112 9 43     SPACE eurjchem-112 9 44 these these DET eurjchem-112 9 45     SPACE eurjchem-112 9 46 compounds compound VERB eurjchem-112 9 47     SPACE eurjchem-112 9 48 using use VERB eurjchem-112 9 49     SPACE eurjchem-112 9 50 more more ADJ eurjchem-112 9 51     SPACE eurjchem-112 9 52 efficient efficient ADJ eurjchem-112 9 53 , , PUNCT eurjchem-112 9 54     SPACE eurjchem-112 9 55 convenient convenient ADJ eurjchem-112 9 56     SPACE eurjchem-112 9 57 and and CCONJ eurjchem-112 9 58     SPACE eurjchem-112 9 59 green green ADJ eurjchem-112 9 60     SPACE eurjchem-112 9 61 conditions condition NOUN eurjchem-112 9 62     SPACE eurjchem-112 9 63 even even ADV eurjchem-112 9 64     SPACE eurjchem-112 9 65 safer safe ADJ eurjchem-112 9 66     SPACE eurjchem-112 9 67 precursors precursor NOUN eurjchem-112 9 68 . . PUNCT eurjchem-112 9 69     SPACE eurjchem-112 9 70 in in ADP eurjchem-112 9 71     SPACE eurjchem-112 9 72 this this DET eurjchem-112 9 73     SPACE eurjchem-112 9 74 context context NOUN eurjchem-112 9 75 , , PUNCT eurjchem-112 9 76     SPACE eurjchem-112 9 77 multi multi ADJ eurjchem-112 9 78     SPACE eurjchem-112 9 79 component component NOUN eurjchem-112 9 80     SPACE eurjchem-112 9 81 reactions reaction NOUN eurjchem-112 9 82     SPACE eurjchem-112 9 83 ( ( PUNCT eurjchem-112 9 84 mcrs mcrs PROPN eurjchem-112 9 85 ) ) PUNCT eurjchem-112 9 86     SPACE eurjchem-112 9 87 have have AUX eurjchem-112 9 88     SPACE eurjchem-112 9 89 played play VERB eurjchem-112 9 90     SPACE eurjchem-112 9 91 an an DET eurjchem-112 9 92     SPACE eurjchem-112 9 93 important important ADJ eurjchem-112 9 94     SPACE eurjchem-112 9 95 role role NOUN eurjchem-112 9 96     SPACE eurjchem-112 9 97 in in ADP eurjchem-112 9 98     SPACE eurjchem-112 9 99 these these DET eurjchem-112 9 100     SPACE eurjchem-112 9 101 processes process NOUN eurjchem-112 9 102     SPACE eurjchem-112 9 103 [ [ X eurjchem-112 9 104 7 7 NUM eurjchem-112 9 105 ] ] PUNCT eurjchem-112 9 106 . . PUNCT eurjchem-112 9 107     SPACE eurjchem-112 9 108 mcrs mcrs PROPN eurjchem-112 9 109     SPACE eurjchem-112 9 110 in in ADP eurjchem-112 9 111     SPACE eurjchem-112 9 112 which which PRON eurjchem-112 9 113     SPACE eurjchem-112 9 114 at at ADP eurjchem-112 9 115     SPACE eurjchem-112 9 116 least least ADJ eurjchem-112 9 117     SPACE eurjchem-112 9 118 three three NUM eurjchem-112 9 119     SPACE eurjchem-112 9 120 starting start VERB eurjchem-112 9 121     SPACE eurjchem-112 9 122 materials material NOUN eurjchem-112 9 123     SPACE eurjchem-112 9 124 react react VERB eurjchem-112 9 125     SPACE eurjchem-112 9 126 together together ADV eurjchem-112 9 127     SPACE eurjchem-112 9 128 in in ADP eurjchem-112 9 129     SPACE eurjchem-112 9 130 one one NUM eurjchem-112 9 131     SPACE eurjchem-112 9 132 pot pot NOUN eurjchem-112 9 133     SPACE eurjchem-112 9 134 to to PART eurjchem-112 9 135     SPACE eurjchem-112 9 136 give give VERB eurjchem-112 9 137     SPACE eurjchem-112 9 138 a a DET eurjchem-112 9 139     SPACE eurjchem-112 9 140 product product NOUN eurjchem-112 9 141 , , PUNCT eurjchem-112 9 142     SPACE eurjchem-112 9 143 is be AUX eurjchem-112 9 144     SPACE eurjchem-112 9 145 in in ADP eurjchem-112 9 146     SPACE eurjchem-112 9 147 contrast contrast NOUN eurjchem-112 9 148     SPACE eurjchem-112 9 149 to to ADP eurjchem-112 9 150     SPACE eurjchem-112 9 151 classical classical ADJ eurjchem-112 9 152     SPACE eurjchem-112 9 153 multi‐step multi‐step NOUN eurjchem-112 9 154     SPACE eurjchem-112 9 155 reactions reaction NOUN eurjchem-112 9 156 , , PUNCT eurjchem-112 9 157     SPACE eurjchem-112 9 158 where where SCONJ eurjchem-112 9 159     SPACE eurjchem-112 9 160 only only ADV eurjchem-112 9 161     SPACE eurjchem-112 9 162 two two NUM eurjchem-112 9 163     SPACE eurjchem-112 9 164 starting start VERB eurjchem-112 9 165     SPACE eurjchem-112 9 166 materials material NOUN eurjchem-112 9 167     SPACE eurjchem-112 9 168 react react VERB eurjchem-112 9 169 . . PUNCT eurjchem-112 9 170     SPACE eurjchem-112 10 1 whenever whenever SCONJ eurjchem-112 10 2     SPACE eurjchem-112 10 3 an an DET eurjchem-112 10 4     SPACE eurjchem-112 10 5 mcr mcr NOUN eurjchem-112 10 6     SPACE eurjchem-112 10 7 can can AUX eurjchem-112 10 8     SPACE eurjchem-112 10 9 be be AUX eurjchem-112 10 10     SPACE eurjchem-112 10 11 applied apply VERB eurjchem-112 10 12     SPACE eurjchem-112 10 13 in in ADP eurjchem-112 10 14     SPACE eurjchem-112 10 15 chemistry chemistry NOUN eurjchem-112 10 16 , , PUNCT eurjchem-112 10 17     SPACE eurjchem-112 10 18 this this PRON eurjchem-112 10 19     SPACE eurjchem-112 10 20 is be AUX eurjchem-112 10 21     SPACE eurjchem-112 10 22 preferred preferred ADJ eurjchem-112 10 23     SPACE eurjchem-112 10 24 since since SCONJ eurjchem-112 10 25     SPACE eurjchem-112 10 26 it it PRON eurjchem-112 10 27     SPACE eurjchem-112 10 28 is be AUX eurjchem-112 10 29     SPACE eurjchem-112 10 30 easier easy ADJ eurjchem-112 10 31     SPACE eurjchem-112 10 32 to to PART eurjchem-112 10 33     SPACE eurjchem-112 10 34 perform perform VERB eurjchem-112 10 35 , , PUNCT eurjchem-112 10 36     SPACE eurjchem-112 10 37 gives give VERB eurjchem-112 10 38     SPACE eurjchem-112 10 39 higher high ADJ eurjchem-112 10 40     SPACE eurjchem-112 10 41 yields yield NOUN eurjchem-112 10 42     SPACE eurjchem-112 10 43 and and CCONJ eurjchem-112 10 44     SPACE eurjchem-112 10 45 is be AUX eurjchem-112 10 46     SPACE eurjchem-112 10 47 less less ADJ eurjchem-112 10 48     SPACE eurjchem-112 10 49 time time NOUN eurjchem-112 10 50     SPACE eurjchem-112 10 51 consuming consume VERB eurjchem-112 10 52     SPACE eurjchem-112 11 1 [ [ X eurjchem-112 11 2 8 8 NUM eurjchem-112 11 3 ] ] PUNCT eurjchem-112 11 4 . . PUNCT eurjchem-112 11 5     SPACE eurjchem-112 11 6 therefore therefore ADV eurjchem-112 11 7 , , PUNCT eurjchem-112 11 8     SPACE eurjchem-112 11 9 we we PRON eurjchem-112 11 10     SPACE eurjchem-112 11 11 decided decide VERB eurjchem-112 11 12     SPACE eurjchem-112 11 13 to to PART eurjchem-112 11 14     SPACE eurjchem-112 11 15 use use VERB eurjchem-112 11 16     SPACE eurjchem-112 11 17 mcr mcr PROPN eurjchem-112 11 18     SPACE eurjchem-112 11 19 for for ADP eurjchem-112 11 20     SPACE eurjchem-112 11 21 the the DET eurjchem-112 11 22     SPACE eurjchem-112 11 23 synthesis synthesis NOUN eurjchem-112 11 24     SPACE eurjchem-112 11 25 of of ADP eurjchem-112 11 26     SPACE eurjchem-112 11 27 3‐cyano‐pyridines 3‐cyano‐pyridine NOUN eurjchem-112 11 28 . . PUNCT eurjchem-112 11 29     SPACE eurjchem-112 12 1 we we PRON eurjchem-112 12 2     SPACE eurjchem-112 12 3 wish wish VERB eurjchem-112 12 4     SPACE eurjchem-112 12 5 to to PART eurjchem-112 12 6     SPACE eurjchem-112 12 7 introduce introduce VERB eurjchem-112 12 8     SPACE eurjchem-112 12 9 this this DET eurjchem-112 12 10     SPACE eurjchem-112 12 11 procedure procedure NOUN eurjchem-112 12 12     SPACE eurjchem-112 12 13 as as ADP eurjchem-112 12 14     SPACE eurjchem-112 12 15 a a DET eurjchem-112 12 16     SPACE eurjchem-112 12 17 mild mild ADJ eurjchem-112 12 18 , , PUNCT eurjchem-112 12 19     SPACE eurjchem-112 12 20 practical practical ADJ eurjchem-112 12 21     SPACE eurjchem-112 12 22 and and CCONJ eurjchem-112 12 23     SPACE eurjchem-112 12 24 highly highly ADV eurjchem-112 12 25     SPACE eurjchem-112 12 26 efficient efficient ADJ eurjchem-112 12 27     SPACE eurjchem-112 12 28 reaction reaction NOUN eurjchem-112 12 29     SPACE eurjchem-112 12 30 for for ADP eurjchem-112 12 31     SPACE eurjchem-112 12 32 the the DET eurjchem-112 12 33     SPACE eurjchem-112 12 34 preparation preparation NOUN eurjchem-112 12 35     SPACE eurjchem-112 12 36 of of ADP eurjchem-112 12 37     SPACE eurjchem-112 12 38 these these DET eurjchem-112 12 39     SPACE eurjchem-112 12 40 compounds compound VERB eurjchem-112 12 41     SPACE eurjchem-112 12 42 using use VERB eurjchem-112 12 43     SPACE eurjchem-112 12 44 1,4‐diaza‐bicyclo[2,2,2]octane 1,4‐diaza‐bicyclo[2,2,2]octane NUM eurjchem-112 12 45     SPACE eurjchem-112 12 46 ( ( PUNCT eurjchem-112 12 47 dabco dabco NOUN eurjchem-112 12 48 ) ) PUNCT eurjchem-112 12 49     SPACE eurjchem-112 12 50 as as ADP eurjchem-112 12 51     SPACE eurjchem-112 12 52 a a DET eurjchem-112 12 53     SPACE eurjchem-112 12 54 catalyst catalyst NOUN eurjchem-112 12 55     SPACE eurjchem-112 12 56 under under ADP eurjchem-112 12 57     SPACE eurjchem-112 12 58 refluxing refluxing NOUN eurjchem-112 12 59     SPACE eurjchem-112 12 60 conditions condition NOUN eurjchem-112 12 61     SPACE eurjchem-112 12 62 ( ( PUNCT eurjchem-112 12 63 scheme scheme NOUN eurjchem-112 12 64     SPACE eurjchem-112 12 65 1 1 NUM eurjchem-112 12 66 ) ) PUNCT eurjchem-112 12 67 . . PUNCT eurjchem-112 12 68         SPACE eurjchem-112 13 1 scheme scheme NOUN eurjchem-112 13 2     SPACE eurjchem-112 13 3 1 1 NUM eurjchem-112 13 4         SPACE eurjchem-112 13 5 2 2 NUM eurjchem-112 13 6 . . PUNCT eurjchem-112 13 7     SPACE eurjchem-112 14 1 experimental experimental ADJ eurjchem-112 14 2         SPACE eurjchem-112 14 3 all all PRON eurjchem-112 14 4     SPACE eurjchem-112 14 5 the the DET eurjchem-112 14 6     SPACE eurjchem-112 14 7 chemicals chemical NOUN eurjchem-112 14 8     SPACE eurjchem-112 14 9 were be AUX eurjchem-112 14 10     SPACE eurjchem-112 14 11 obtained obtain VERB eurjchem-112 14 12     SPACE eurjchem-112 14 13 from from ADP eurjchem-112 14 14     SPACE eurjchem-112 14 15 merck merck NOUN eurjchem-112 14 16     SPACE eurjchem-112 14 17 company company NOUN eurjchem-112 14 18     SPACE eurjchem-112 14 19 and and CCONJ eurjchem-112 14 20     SPACE eurjchem-112 14 21 used use VERB eurjchem-112 14 22     SPACE eurjchem-112 14 23 as as SCONJ eurjchem-112 14 24     SPACE eurjchem-112 14 25 received receive VERB eurjchem-112 14 26 . . PUNCT eurjchem-112 14 27     SPACE eurjchem-112 15 1 all all DET eurjchem-112 15 2     SPACE eurjchem-112 15 3 products product NOUN eurjchem-112 15 4     SPACE eurjchem-112 15 5 are be AUX eurjchem-112 15 6     SPACE eurjchem-112 15 7 known know VERB eurjchem-112 15 8     SPACE eurjchem-112 15 9 compounds compound NOUN eurjchem-112 15 10     SPACE eurjchem-112 15 11 and and CCONJ eurjchem-112 15 12     SPACE eurjchem-112 15 13 were be AUX eurjchem-112 15 14     SPACE eurjchem-112 15 15 characterized characterize VERB eurjchem-112 15 16     SPACE eurjchem-112 15 17 by by ADP eurjchem-112 15 18     SPACE eurjchem-112 15 19 mp mp PROPN eurjchem-112 15 20 , , PUNCT eurjchem-112 15 21     SPACE eurjchem-112 15 22 ir ir PROPN eurjchem-112 15 23 , , PUNCT eurjchem-112 15 24     SPACE eurjchem-112 15 25 1h 1h NUM eurjchem-112 15 26     SPACE eurjchem-112 15 27 nmr nmr NOUN eurjchem-112 15 28     SPACE eurjchem-112 15 29 and and CCONJ eurjchem-112 15 30     SPACE eurjchem-112 15 31 gc gc PROPN eurjchem-112 15 32 / / SYM eurjchem-112 15 33 ms ms PROPN eurjchem-112 15 34 . . PROPN eurjchem-112 15 35     SPACE eurjchem-112 15 36 melting melting NOUN eurjchem-112 15 37     SPACE eurjchem-112 15 38 points point NOUN eurjchem-112 15 39     SPACE eurjchem-112 15 40 were be AUX eurjchem-112 15 41     SPACE eurjchem-112 15 42 measured measure VERB eurjchem-112 15 43     SPACE eurjchem-112 15 44 by by ADP eurjchem-112 15 45     SPACE eurjchem-112 15 46 using use VERB eurjchem-112 15 47     SPACE eurjchem-112 15 48 the the DET eurjchem-112 15 49     SPACE eurjchem-112 15 50 capillary capillary ADJ eurjchem-112 15 51     SPACE eurjchem-112 15 52 tube tube NOUN eurjchem-112 15 53     SPACE eurjchem-112 15 54 method method NOUN eurjchem-112 15 55     SPACE eurjchem-112 15 56 with with ADP eurjchem-112 15 57     SPACE eurjchem-112 15 58 an an DET eurjchem-112 15 59     SPACE eurjchem-112 15 60 electro electro ADJ eurjchem-112 15 61     SPACE eurjchem-112 15 62 thermal thermal ADJ eurjchem-112 15 63     SPACE eurjchem-112 15 64 9200 9200 NUM eurjchem-112 15 65     SPACE eurjchem-112 15 66 apparatus apparatus NOUN eurjchem-112 15 67 . . PUNCT eurjchem-112 15 68     SPACE eurjchem-112 15 69 1h 1h NUM eurjchem-112 15 70     SPACE eurjchem-112 15 71 nmr nmr NOUN eurjchem-112 15 72     SPACE eurjchem-112 15 73 spectra spectra NOUN eurjchem-112 15 74     SPACE eurjchem-112 15 75 were be AUX eurjchem-112 15 76     SPACE eurjchem-112 15 77 recorded record VERB eurjchem-112 15 78     SPACE eurjchem-112 15 79 on on ADP eurjchem-112 15 80     SPACE eurjchem-112 15 81 a a DET eurjchem-112 15 82     SPACE eurjchem-112 15 83 bruker bruker NOUN eurjchem-112 15 84     SPACE eurjchem-112 15 85 aqs aqs PROPN eurjchem-112 15 86     SPACE eurjchem-112 15 87 avance‐300 avance‐300 ADJ eurjchem-112 15 88     SPACE eurjchem-112 15 89 mhz mhz NOUN eurjchem-112 15 90     SPACE eurjchem-112 15 91 spectrometer spectrometer NOUN eurjchem-112 15 92     SPACE eurjchem-112 15 93 using use VERB eurjchem-112 15 94     SPACE eurjchem-112 15 95 tms tms NOUN eurjchem-112 15 96     SPACE eurjchem-112 15 97 as as ADP eurjchem-112 15 98     SPACE eurjchem-112 15 99 an an DET eurjchem-112 15 100     SPACE eurjchem-112 15 101 internal internal ADJ eurjchem-112 15 102     SPACE eurjchem-112 15 103 standard standard NOUN eurjchem-112 15 104     SPACE eurjchem-112 15 105 ( ( PUNCT eurjchem-112 15 106 cdcl3 cdcl3 NOUN eurjchem-112 15 107     SPACE eurjchem-112 15 108 solution solution NOUN eurjchem-112 15 109 ) ) PUNCT eurjchem-112 15 110 . . PUNCT eurjchem-112 15 111     SPACE eurjchem-112 16 1 ir ir PROPN eurjchem-112 16 2     SPACE eurjchem-112 16 3 spectra spectra NOUN eurjchem-112 16 4     SPACE eurjchem-112 16 5 were be AUX eurjchem-112 16 6     SPACE eurjchem-112 16 7 recorded record VERB eurjchem-112 16 8     SPACE eurjchem-112 16 9 from from ADP eurjchem-112 16 10     SPACE eurjchem-112 16 11 kbr kbr PROPN eurjchem-112 16 12     SPACE eurjchem-112 16 13 disk disk NOUN eurjchem-112 16 14     SPACE eurjchem-112 16 15 on on ADP eurjchem-112 16 16     SPACE eurjchem-112 16 17 the the DET eurjchem-112 16 18     SPACE eurjchem-112 16 19 ft‐ir ft‐ir ADJ eurjchem-112 16 20     SPACE eurjchem-112 16 21 bruker bruker PROPN eurjchem-112 16 22     SPACE eurjchem-112 16 23 tensor tensor NOUN eurjchem-112 16 24     SPACE eurjchem-112 16 25 27 27 NUM eurjchem-112 16 26 . . PUNCT eurjchem-112 16 27     SPACE eurjchem-112 16 28 gc gc PROPN eurjchem-112 16 29 / / SYM eurjchem-112 16 30 ms ms NOUN eurjchem-112 16 31     SPACE eurjchem-112 16 32 spectra spectra NOUN eurjchem-112 16 33     SPACE eurjchem-112 16 34 were be AUX eurjchem-112 16 35     SPACE eurjchem-112 16 36 recorded record VERB eurjchem-112 16 37     SPACE eurjchem-112 16 38 on on ADP eurjchem-112 16 39     SPACE eurjchem-112 16 40 an an DET eurjchem-112 16 41     SPACE eurjchem-112 16 42 agilent agilent PROPN eurjchem-112 16 43     SPACE eurjchem-112 16 44 technologies technology NOUN eurjchem-112 16 45     SPACE eurjchem-112 16 46 6890 6890 NUM eurjchem-112 16 47     SPACE eurjchem-112 16 48 network network NOUN eurjchem-112 16 49     SPACE eurjchem-112 16 50 gc gc PROPN eurjchem-112 16 51     SPACE eurjchem-112 16 52 system system NOUN eurjchem-112 16 53     SPACE eurjchem-112 16 54 and and CCONJ eurjchem-112 16 55     SPACE eurjchem-112 16 56 an an DET eurjchem-112 16 57     SPACE eurjchem-112 16 58 agilent agilent PROPN eurjchem-112 16 59     SPACE eurjchem-112 16 60 5973 5973 NUM eurjchem-112 16 61     SPACE eurjchem-112 16 62 network network NOUN eurjchem-112 16 63     SPACE eurjchem-112 16 64 mass mass ADJ eurjchem-112 16 65     SPACE eurjchem-112 16 66 selective selective ADJ eurjchem-112 16 67     SPACE eurjchem-112 16 68 detector detector NOUN eurjchem-112 16 69 . . PUNCT eurjchem-112 16 70     SPACE eurjchem-112 17 1 thin thin ADJ eurjchem-112 17 2     SPACE eurjchem-112 17 3 layer layer NOUN eurjchem-112 17 4     SPACE eurjchem-112 17 5 chromatography chromatography NOUN eurjchem-112 17 6     SPACE eurjchem-112 17 7 ( ( PUNCT eurjchem-112 17 8 tlc tlc NOUN eurjchem-112 17 9 ) ) PUNCT eurjchem-112 17 10     SPACE eurjchem-112 17 11 on on ADP eurjchem-112 17 12     SPACE eurjchem-112 17 13 commercial commercial ADJ eurjchem-112 17 14     SPACE eurjchem-112 17 15 aluminum‐packed aluminum‐packe VERB eurjchem-112 17 16     SPACE eurjchem-112 17 17 plates plate NOUN eurjchem-112 17 18     SPACE eurjchem-112 17 19 of of ADP eurjchem-112 17 20     SPACE eurjchem-112 17 21 silica silica NOUN eurjchem-112 17 22     SPACE eurjchem-112 17 23 gel gel NOUN eurjchem-112 17 24 , , PUNCT eurjchem-112 17 25     SPACE eurjchem-112 17 26 60 60 NUM eurjchem-112 17 27     SPACE eurjchem-112 17 28 f254 f254 PROPN eurjchem-112 17 29     SPACE eurjchem-112 17 30 was be AUX eurjchem-112 17 31     SPACE eurjchem-112 17 32 used use VERB eurjchem-112 17 33     SPACE eurjchem-112 17 34 to to PART eurjchem-112 17 35     SPACE eurjchem-112 17 36 monitor monitor VERB eurjchem-112 17 37     SPACE eurjchem-112 17 38 the the DET eurjchem-112 17 39     SPACE eurjchem-112 17 40 progress progress NOUN eurjchem-112 17 41     SPACE eurjchem-112 17 42 of of ADP eurjchem-112 17 43     SPACE eurjchem-112 17 44 reactions reaction NOUN eurjchem-112 17 45 . . PUNCT eurjchem-112 17 46             SPACE eurjchem-112 17 47 2.1 2.1 NUM eurjchem-112 17 48 . . PUNCT eurjchem-112 17 49     SPACE eurjchem-112 17 50 typical typical ADJ eurjchem-112 17 51     SPACE eurjchem-112 17 52 procedure procedure NOUN eurjchem-112 17 53     SPACE eurjchem-112 17 54 for for ADP eurjchem-112 17 55     SPACE eurjchem-112 17 56 preparation preparation NOUN eurjchem-112 17 57     SPACE eurjchem-112 17 58 of of ADP eurjchem-112 17 59     SPACE eurjchem-112 17 60 4­aryl(alkyl)­6­ 4­aryl(alkyl)­6­ NOUN eurjchem-112 17 61 ( ( PUNCT eurjchem-112 17 62 3,4­dimethoxyphenyl)­3­cyano­2(1h)­iminopyridines 3,4­dimethoxyphenyl)­3­cyano­2(1h)­iminopyridine NOUN eurjchem-112 17 63     SPACE eurjchem-112 17 64 ( ( PUNCT eurjchem-112 17 65 5a­e 5a­e NUM eurjchem-112 17 66 ) ) PUNCT eurjchem-112 17 67         SPACE eurjchem-112 17 68 a a DET eurjchem-112 17 69     SPACE eurjchem-112 17 70 mixture mixture NOUN eurjchem-112 17 71     SPACE eurjchem-112 17 72 of of ADP eurjchem-112 17 73     SPACE eurjchem-112 17 74 3,4‐dimethoxyacetophenone 3,4‐dimethoxyacetophenone NOUN eurjchem-112 17 75     SPACE eurjchem-112 17 76 ( ( PUNCT eurjchem-112 17 77 1 1 NUM eurjchem-112 17 78     SPACE eurjchem-112 17 79 mmol mmol NOUN eurjchem-112 17 80 ) ) PUNCT eurjchem-112 17 81 , , PUNCT eurjchem-112 17 82     SPACE eurjchem-112 17 83 malononitrile malononitrile NOUN eurjchem-112 17 84     SPACE eurjchem-112 17 85 ( ( PUNCT eurjchem-112 17 86 1 1 NUM eurjchem-112 17 87     SPACE eurjchem-112 17 88 mmol mmol NOUN eurjchem-112 17 89 ) ) PUNCT eurjchem-112 17 90 , , PUNCT eurjchem-112 17 91     SPACE eurjchem-112 17 92 the the DET eurjchem-112 17 93     SPACE eurjchem-112 17 94 appropriate appropriate ADJ eurjchem-112 17 95     SPACE eurjchem-112 17 96 aldehyde aldehyde NOUN eurjchem-112 17 97     SPACE eurjchem-112 17 98 ( ( PUNCT eurjchem-112 17 99 1 1 NUM eurjchem-112 17 100     SPACE eurjchem-112 17 101 mmol mmol NOUN eurjchem-112 17 102 ) ) PUNCT eurjchem-112 17 103 , , PUNCT eurjchem-112 17 104     SPACE eurjchem-112 17 105 ammonium ammonium NOUN eurjchem-112 17 106     SPACE eurjchem-112 17 107 acetate acetate NOUN eurjchem-112 17 108     SPACE eurjchem-112 17 109 ( ( PUNCT eurjchem-112 17 110 8 8 NUM eurjchem-112 17 111     SPACE eurjchem-112 17 112 mmol mmol NOUN eurjchem-112 17 113 ) ) PUNCT eurjchem-112 17 114     SPACE eurjchem-112 17 115 and and CCONJ eurjchem-112 17 116     SPACE eurjchem-112 17 117 dabco dabco PROPN eurjchem-112 17 118     SPACE eurjchem-112 17 119 ( ( PUNCT eurjchem-112 17 120 5mol 5mol NOUN eurjchem-112 17 121     SPACE eurjchem-112 17 122 % % NOUN eurjchem-112 17 123 ) ) PUNCT eurjchem-112 17 124     SPACE eurjchem-112 17 125 in in ADP eurjchem-112 17 126     SPACE eurjchem-112 17 127 ethanol ethanol NOUN eurjchem-112 17 128     SPACE eurjchem-112 17 129 beheshtia beheshtia PROPN eurjchem-112 17 130     SPACE eurjchem-112 17 131 et et PROPN eurjchem-112 17 132     SPACE eurjchem-112 17 133 al al PROPN eurjchem-112 17 134 . . PROPN eurjchem-112 17 135     SPACE eurjchem-112 17 136 / / SYM eurjchem-112 17 137     SPACE eurjchem-112 17 138 european european ADJ eurjchem-112 17 139     SPACE eurjchem-112 17 140 journal journal NOUN eurjchem-112 17 141     SPACE eurjchem-112 17 142 of of ADP eurjchem-112 17 143     SPACE eurjchem-112 17 144 chemistry chemistry NOUN eurjchem-112 17 145     SPACE eurjchem-112 17 146 1 1 NUM eurjchem-112 17 147     SPACE eurjchem-112 17 148 ( ( PUNCT eurjchem-112 17 149 3 3 NUM eurjchem-112 17 150 ) ) PUNCT eurjchem-112 17 151     SPACE eurjchem-112 17 152 ( ( PUNCT eurjchem-112 17 153 2010 2010 NUM eurjchem-112 17 154 ) ) PUNCT eurjchem-112 17 155     SPACE eurjchem-112 17 156 232­235 232­235 NUM eurjchem-112 17 157     SPACE eurjchem-112 17 158 233 233 NUM eurjchem-112 17 159           SPACE eurjchem-112 17 160 table table NOUN eurjchem-112 17 161     SPACE eurjchem-112 17 162 1 1 NUM eurjchem-112 17 163 . . PUNCT eurjchem-112 17 164     SPACE eurjchem-112 17 165 synthesis synthesis NOUN eurjchem-112 17 166     SPACE eurjchem-112 17 167 of of ADP eurjchem-112 17 168     SPACE eurjchem-112 17 169 3‐cyanopyridines 3‐cyanopyridine NOUN eurjchem-112 17 170     SPACE eurjchem-112 17 171 derivatives derivative NOUN eurjchem-112 17 172     SPACE eurjchem-112 17 173 catalyzed catalyze VERB eurjchem-112 17 174     SPACE eurjchem-112 17 175 by by ADP eurjchem-112 17 176     SPACE eurjchem-112 17 177 dabco dabco PROPN eurjchem-112 17 178 . . PUNCT eurjchem-112 17 179     SPACE eurjchem-112 18 1 entry entry NOUN eurjchem-112 18 2     SPACE eurjchem-112 18 3 r r NOUN eurjchem-112 18 4     SPACE eurjchem-112 18 5 x x NOUN eurjchem-112 18 6     SPACE eurjchem-112 18 7 z z NOUN eurjchem-112 18 8     SPACE eurjchem-112 18 9 product product NOUN eurjchem-112 18 10     SPACE eurjchem-112 18 11 time time NOUN eurjchem-112 18 12     SPACE eurjchem-112 18 13 ( ( PUNCT eurjchem-112 18 14 h h NOUN eurjchem-112 18 15 ) ) PUNCT eurjchem-112 18 16     SPACE eurjchem-112 18 17 yield yield NOUN eurjchem-112 18 18     SPACE eurjchem-112 18 19 ( ( PUNCT eurjchem-112 18 20 % % NOUN eurjchem-112 18 21 ) ) PUNCT eurjchem-112 18 22 a a DET eurjchem-112 18 23                         SPACE eurjchem-112 18 24 25˚c 25˚c NUM eurjchem-112 18 25                                             SPACE eurjchem-112 18 26 45˚c 45˚c NUM eurjchem-112 18 27                                             SPACE eurjchem-112 18 28 78˚c 78˚c NUM eurjchem-112 18 29     SPACE eurjchem-112 18 30 1 1 NUM eurjchem-112 18 31     SPACE eurjchem-112 18 32 -ch3 -ch3 PROPN eurjchem-112 18 33 cn cn PROPN eurjchem-112 18 34     SPACE eurjchem-112 18 35 nh nh PROPN eurjchem-112 18 36     SPACE eurjchem-112 18 37 5a 5a NUM eurjchem-112 18 38     SPACE eurjchem-112 18 39 2 2 NUM eurjchem-112 18 40     SPACE eurjchem-112 18 41 45 45 NUM eurjchem-112 18 42     SPACE eurjchem-112 18 43 65 65 NUM eurjchem-112 18 44     SPACE eurjchem-112 18 45 87 87 NUM eurjchem-112 18 46     SPACE eurjchem-112 18 47 2 2 NUM eurjchem-112 18 48         SPACE eurjchem-112 18 49 cn cn PROPN eurjchem-112 18 50     SPACE eurjchem-112 18 51 nh nh PROPN eurjchem-112 18 52     SPACE eurjchem-112 18 53 5b 5b NOUN eurjchem-112 18 54     SPACE eurjchem-112 18 55 2 2 NUM eurjchem-112 18 56     SPACE eurjchem-112 18 57 45 45 NUM eurjchem-112 18 58     SPACE eurjchem-112 18 59 70 70 NUM eurjchem-112 18 60     SPACE eurjchem-112 18 61 91 91 NUM eurjchem-112 18 62     SPACE eurjchem-112 18 63 3 3 NUM eurjchem-112 18 64         SPACE eurjchem-112 18 65 cn cn PROPN eurjchem-112 18 66     SPACE eurjchem-112 18 67 nh nh PROPN eurjchem-112 18 68     SPACE eurjchem-112 18 69 5c 5c NOUN eurjchem-112 18 70     SPACE eurjchem-112 18 71 2 2 NUM eurjchem-112 18 72     SPACE eurjchem-112 18 73 40 40 NUM eurjchem-112 18 74     SPACE eurjchem-112 18 75 68 68 NUM eurjchem-112 18 76     SPACE eurjchem-112 18 77 90 90 NUM eurjchem-112 18 78     SPACE eurjchem-112 18 79 4 4 NUM eurjchem-112 18 80         SPACE eurjchem-112 18 81 cn cn PROPN eurjchem-112 18 82     SPACE eurjchem-112 18 83 nh nh PROPN eurjchem-112 18 84     SPACE eurjchem-112 18 85 5d 5d PROPN eurjchem-112 18 86     SPACE eurjchem-112 18 87 2 2 NUM eurjchem-112 18 88     SPACE eurjchem-112 18 89 45 45 NUM eurjchem-112 18 90     SPACE eurjchem-112 18 91 72 72 NUM eurjchem-112 18 92     SPACE eurjchem-112 18 93 88 88 NUM eurjchem-112 18 94     SPACE eurjchem-112 18 95 5 5 NUM eurjchem-112 18 96     SPACE eurjchem-112 18 97 cn cn PROPN eurjchem-112 18 98     SPACE eurjchem-112 18 99 nh nh PROPN eurjchem-112 18 100     SPACE eurjchem-112 18 101 5e 5e NOUN eurjchem-112 18 102     SPACE eurjchem-112 18 103 2 2 NUM eurjchem-112 18 104     SPACE eurjchem-112 18 105 50 50 NUM eurjchem-112 18 106     SPACE eurjchem-112 18 107 71 71 NUM eurjchem-112 18 108     SPACE eurjchem-112 18 109 89 89 NUM eurjchem-112 18 110     SPACE eurjchem-112 18 111 6 6 NUM eurjchem-112 18 112     SPACE eurjchem-112 18 113 -ch3 -ch3 NUM eurjchem-112 18 114 cooet cooet NOUN eurjchem-112 18 115     SPACE eurjchem-112 18 116 o o NOUN eurjchem-112 18 117     SPACE eurjchem-112 18 118 6a 6a NOUN eurjchem-112 18 119     SPACE eurjchem-112 18 120 2 2 NUM eurjchem-112 18 121     SPACE eurjchem-112 18 122 45 45 NUM eurjchem-112 18 123     SPACE eurjchem-112 18 124 65 65 NUM eurjchem-112 18 125     SPACE eurjchem-112 18 126 88 88 NUM eurjchem-112 18 127     SPACE eurjchem-112 18 128 7 7 NUM eurjchem-112 18 129         SPACE eurjchem-112 18 130 cooet cooet NOUN eurjchem-112 18 131     SPACE eurjchem-112 18 132 o o NOUN eurjchem-112 18 133     SPACE eurjchem-112 18 134 6b 6b NOUN eurjchem-112 18 135     SPACE eurjchem-112 18 136 2 2 NUM eurjchem-112 18 137     SPACE eurjchem-112 18 138 45 45 NUM eurjchem-112 18 139     SPACE eurjchem-112 18 140 72 72 NUM eurjchem-112 18 141     SPACE eurjchem-112 18 142 94 94 NUM eurjchem-112 18 143     SPACE eurjchem-112 18 144 8 8 NUM eurjchem-112 18 145         SPACE eurjchem-112 18 146 cooet cooet NOUN eurjchem-112 18 147     SPACE eurjchem-112 18 148 o o NOUN eurjchem-112 18 149     SPACE eurjchem-112 18 150 6c 6c NOUN eurjchem-112 18 151     SPACE eurjchem-112 18 152 2 2 NUM eurjchem-112 18 153     SPACE eurjchem-112 18 154 40 40 NUM eurjchem-112 18 155     SPACE eurjchem-112 18 156 70 70 NUM eurjchem-112 18 157     SPACE eurjchem-112 18 158 90 90 NUM eurjchem-112 18 159     SPACE eurjchem-112 18 160 9 9 NUM eurjchem-112 18 161         SPACE eurjchem-112 18 162 cooet cooet NOUN eurjchem-112 18 163     SPACE eurjchem-112 18 164 o o NOUN eurjchem-112 18 165     SPACE eurjchem-112 18 166 6d 6d NOUN eurjchem-112 18 167     SPACE eurjchem-112 18 168 2 2 NUM eurjchem-112 18 169     SPACE eurjchem-112 18 170 45 45 NUM eurjchem-112 18 171     SPACE eurjchem-112 18 172 72 72 NUM eurjchem-112 18 173     SPACE eurjchem-112 18 174 88 88 NUM eurjchem-112 18 175     SPACE eurjchem-112 18 176 10 10 NUM eurjchem-112 18 177     SPACE eurjchem-112 18 178 cooet cooet NOUN eurjchem-112 18 179     SPACE eurjchem-112 18 180 o o NOUN eurjchem-112 18 181     SPACE eurjchem-112 18 182 6e 6e NOUN eurjchem-112 18 183     SPACE eurjchem-112 18 184 2 2 NUM eurjchem-112 18 185     SPACE eurjchem-112 18 186 50 50 NUM eurjchem-112 18 187     SPACE eurjchem-112 18 188 75 75 NUM eurjchem-112 18 189     SPACE eurjchem-112 18 190 89 89 NUM eurjchem-112 18 191     SPACE eurjchem-112 18 192 ayield ayield NOUN eurjchem-112 18 193     SPACE eurjchem-112 18 194 of of ADP eurjchem-112 18 195     SPACE eurjchem-112 18 196 isolated isolated ADJ eurjchem-112 18 197     SPACE eurjchem-112 18 198 products product NOUN eurjchem-112 18 199 . . PUNCT eurjchem-112 18 200             SPACE eurjchem-112 19 1 ( ( PUNCT eurjchem-112 19 2 5 5 NUM eurjchem-112 19 3     SPACE eurjchem-112 19 4 ml ml NOUN eurjchem-112 19 5 ) ) PUNCT eurjchem-112 19 6     SPACE eurjchem-112 19 7 was be AUX eurjchem-112 19 8     SPACE eurjchem-112 19 9 refluxed refluxe VERB eurjchem-112 19 10     SPACE eurjchem-112 19 11 for for ADP eurjchem-112 19 12     SPACE eurjchem-112 19 13 2h 2h NUM eurjchem-112 19 14 . . PUNCT eurjchem-112 19 15     SPACE eurjchem-112 20 1 the the DET eurjchem-112 20 2     SPACE eurjchem-112 20 3 mixture mixture NOUN eurjchem-112 20 4     SPACE eurjchem-112 20 5 was be AUX eurjchem-112 20 6     SPACE eurjchem-112 20 7 cooled cool VERB eurjchem-112 20 8     SPACE eurjchem-112 20 9 to to ADP eurjchem-112 20 10     SPACE eurjchem-112 20 11 room room NOUN eurjchem-112 20 12     SPACE eurjchem-112 20 13 temperature temperature NOUN eurjchem-112 20 14     SPACE eurjchem-112 20 15 and and CCONJ eurjchem-112 20 16     SPACE eurjchem-112 20 17 the the DET eurjchem-112 20 18     SPACE eurjchem-112 20 19 precipitated precipitate VERB eurjchem-112 20 20     SPACE eurjchem-112 20 21 products product NOUN eurjchem-112 20 22     SPACE eurjchem-112 20 23 were be AUX eurjchem-112 20 24     SPACE eurjchem-112 20 25 separated separate VERB eurjchem-112 20 26     SPACE eurjchem-112 20 27 by by ADP eurjchem-112 20 28     SPACE eurjchem-112 20 29 filtration filtration NOUN eurjchem-112 20 30     SPACE eurjchem-112 20 31 then then ADV eurjchem-112 20 32         SPACE eurjchem-112 20 33 washed wash VERB eurjchem-112 20 34     SPACE eurjchem-112 20 35 successively successively ADV eurjchem-112 20 36     SPACE eurjchem-112 20 37 with with ADP eurjchem-112 20 38     SPACE eurjchem-112 20 39 water water NOUN eurjchem-112 20 40 , , PUNCT eurjchem-112 20 41     SPACE eurjchem-112 20 42 dried dry VERB eurjchem-112 20 43     SPACE eurjchem-112 20 44 and and CCONJ eurjchem-112 20 45     SPACE eurjchem-112 20 46 crystallized crystallize VERB eurjchem-112 20 47 . . PUNCT eurjchem-112 20 48           SPACE eurjchem-112 21 1 2.1.2 2.1.2 NUM eurjchem-112 21 2 . . PUNCT eurjchem-112 21 3     SPACE eurjchem-112 21 4 typical typical ADJ eurjchem-112 21 5     SPACE eurjchem-112 21 6 procedure procedure NOUN eurjchem-112 21 7     SPACE eurjchem-112 21 8 for for ADP eurjchem-112 21 9     SPACE eurjchem-112 21 10 preparation preparation NOUN eurjchem-112 21 11     SPACE eurjchem-112 21 12 of of ADP eurjchem-112 21 13     SPACE eurjchem-112 21 14 4­aryl(alkyl)­6­ 4­aryl(alkyl)­6­ NOUN eurjchem-112 21 15 ( ( PUNCT eurjchem-112 21 16 3,4­dimethoxyphenyl)­3­cyano­2(1h)­pyridinones 3,4­dimethoxyphenyl)­3­cyano­2(1h)­pyridinone NOUN eurjchem-112 21 17     SPACE eurjchem-112 21 18 ( ( PUNCT eurjchem-112 21 19 6a­e 6a­e PROPN eurjchem-112 21 20 ) ) PUNCT eurjchem-112 21 21         SPACE eurjchem-112 21 22 the the DET eurjchem-112 21 23     SPACE eurjchem-112 21 24 foregoing foregoing NOUN eurjchem-112 21 25     SPACE eurjchem-112 21 26 method method NOUN eurjchem-112 21 27     SPACE eurjchem-112 21 28 was be AUX eurjchem-112 21 29     SPACE eurjchem-112 21 30 carried carry VERB eurjchem-112 21 31     SPACE eurjchem-112 21 32 out out ADP eurjchem-112 21 33     SPACE eurjchem-112 21 34 except except SCONJ eurjchem-112 21 35     SPACE eurjchem-112 21 36 that that SCONJ eurjchem-112 21 37     SPACE eurjchem-112 21 38 malononitrile malononitrile NOUN eurjchem-112 21 39     SPACE eurjchem-112 21 40 was be AUX eurjchem-112 21 41     SPACE eurjchem-112 21 42 replaced replace VERB eurjchem-112 21 43     SPACE eurjchem-112 21 44 by by ADP eurjchem-112 21 45     SPACE eurjchem-112 21 46 ethyl ethyl PROPN eurjchem-112 21 47     SPACE eurjchem-112 21 48 cyanoacetate cyanoacetate NOUN eurjchem-112 21 49     SPACE eurjchem-112 21 50 ( ( PUNCT eurjchem-112 21 51 table table NOUN eurjchem-112 21 52     SPACE eurjchem-112 21 53 1 1 NUM eurjchem-112 21 54 , , PUNCT eurjchem-112 21 55     SPACE eurjchem-112 21 56 entries entry NOUN eurjchem-112 21 57     SPACE eurjchem-112 21 58 6‐10 6‐10 NUM eurjchem-112 21 59 ) ) PUNCT eurjchem-112 21 60 . . PUNCT eurjchem-112 21 61     SPACE eurjchem-112 21 62 selected select VERB eurjchem-112 21 63     SPACE eurjchem-112 21 64 physical physical ADJ eurjchem-112 21 65     SPACE eurjchem-112 21 66 data datum NOUN eurjchem-112 21 67 : : PUNCT eurjchem-112 21 68       SPACE eurjchem-112 21 69 5a 5a NUM eurjchem-112 21 70 : : PUNCT eurjchem-112 21 71     SPACE eurjchem-112 21 72 m.p m.p PROPN eurjchem-112 21 73 . . PROPN eurjchem-112 21 74 : : PUNCT eurjchem-112 21 75     SPACE eurjchem-112 21 76 213 213 NUM eurjchem-112 21 77     SPACE eurjchem-112 21 78 ºc ºc NOUN eurjchem-112 21 79     SPACE eurjchem-112 21 80 ( ( PUNCT eurjchem-112 21 81 lit light VERB eurjchem-112 21 82 . . PUNCT eurjchem-112 21 83     SPACE eurjchem-112 22 1 212‐214 212‐214 NUM eurjchem-112 22 2     SPACE eurjchem-112 23 1 [ [ X eurjchem-112 23 2 21 21 NUM eurjchem-112 23 3 ] ] PUNCT eurjchem-112 23 4 ) ) PUNCT eurjchem-112 23 5 . . PUNCT eurjchem-112 23 6     SPACE eurjchem-112 24 1 ir ir VERB eurjchem-112 24 2     SPACE eurjchem-112 24 3 ( ( PUNCT eurjchem-112 24 4 kbr kbr PROPN eurjchem-112 24 5 ) ) PUNCT eurjchem-112 24 6     SPACE eurjchem-112 24 7 ( ( PUNCT eurjchem-112 24 8 νmax νmax PROPN eurjchem-112 24 9 , , PUNCT eurjchem-112 24 10     SPACE eurjchem-112 24 11 cm−1 cm−1 NOUN eurjchem-112 24 12 ): ): PUNCT eurjchem-112 24 13     SPACE eurjchem-112 24 14 3513 3513 NUM eurjchem-112 24 15 , , PUNCT eurjchem-112 24 16     SPACE eurjchem-112 24 17 3420 3420 NUM eurjchem-112 24 18 , , PUNCT eurjchem-112 24 19     SPACE eurjchem-112 24 20 2218 2218 NUM eurjchem-112 24 21 . . PUNCT eurjchem-112 24 22     SPACE eurjchem-112 24 23 1h 1h NUM eurjchem-112 24 24     SPACE eurjchem-112 24 25 nmr nmr NOUN eurjchem-112 24 26     SPACE eurjchem-112 24 27 ( ( PUNCT eurjchem-112 24 28 cdcl3 cdcl3 PROPN eurjchem-112 24 29 , , PUNCT eurjchem-112 24 30     SPACE eurjchem-112 24 31 300 300 NUM eurjchem-112 24 32     SPACE eurjchem-112 24 33 mhz mhz NOUN eurjchem-112 24 34 ) ) PUNCT eurjchem-112 24 35     SPACE eurjchem-112 24 36 δh δh NOUN eurjchem-112 24 37     SPACE eurjchem-112 24 38 ( ( PUNCT eurjchem-112 24 39 ppm ppm PROPN eurjchem-112 24 40 ): ): PUNCT eurjchem-112 24 41     SPACE eurjchem-112 24 42 3.65 3.65 NUM eurjchem-112 24 43     SPACE eurjchem-112 24 44 ( ( PUNCT eurjchem-112 24 45 s s PROPN eurjchem-112 24 46 , , PUNCT eurjchem-112 24 47     SPACE eurjchem-112 24 48 3h 3h NUM eurjchem-112 24 49 , , PUNCT eurjchem-112 24 50     SPACE eurjchem-112 24 51 3‐och3 3‐och3 NUM eurjchem-112 24 52 ) ) PUNCT eurjchem-112 24 53 , , PUNCT eurjchem-112 24 54     SPACE eurjchem-112 24 55 3.77 3.77 NUM eurjchem-112 24 56     SPACE eurjchem-112 24 57 ( ( PUNCT eurjchem-112 24 58 s s PROPN eurjchem-112 24 59 , , PUNCT eurjchem-112 24 60     SPACE eurjchem-112 24 61 3h 3h NUM eurjchem-112 24 62 , , PUNCT eurjchem-112 24 63     SPACE eurjchem-112 24 64 4‐och3 4‐och3 NUM eurjchem-112 24 65 ) ) PUNCT eurjchem-112 24 66 , , PUNCT eurjchem-112 24 67     SPACE eurjchem-112 24 68 7.22–7.63 7.22–7.63 NUM eurjchem-112 24 69     SPACE eurjchem-112 24 70 ( ( PUNCT eurjchem-112 24 71 m m PROPN eurjchem-112 24 72 , , PUNCT eurjchem-112 24 73     SPACE eurjchem-112 24 74 9h 9h NOUN eurjchem-112 24 75 , , PUNCT eurjchem-112 24 76     SPACE eurjchem-112 24 77 aromatic aromatic NOUN eurjchem-112 24 78 ) ) PUNCT eurjchem-112 24 79 , , PUNCT eurjchem-112 24 80     SPACE eurjchem-112 24 81 10.48 10.48 NUM eurjchem-112 24 82     SPACE eurjchem-112 24 83 ( ( PUNCT eurjchem-112 24 84 brs br VERB eurjchem-112 24 85 , , PUNCT eurjchem-112 24 86     SPACE eurjchem-112 24 87 1h 1h NUM eurjchem-112 24 88 , , PUNCT eurjchem-112 24 89     SPACE eurjchem-112 24 90 nh nh PROPN eurjchem-112 24 91 ) ) PUNCT eurjchem-112 24 92 , , PUNCT eurjchem-112 24 93     SPACE eurjchem-112 24 94 10.57 10.57 NUM eurjchem-112 24 95     SPACE eurjchem-112 24 96 ( ( PUNCT eurjchem-112 24 97 brs br VERB eurjchem-112 24 98 , , PUNCT eurjchem-112 24 99     SPACE eurjchem-112 24 100 1h 1h NUM eurjchem-112 24 101 , , PUNCT eurjchem-112 24 102     SPACE eurjchem-112 24 103 nh nh PROPN eurjchem-112 24 104 ) ) PUNCT eurjchem-112 24 105 . . PUNCT eurjchem-112 24 106     SPACE eurjchem-112 25 1 ms ms NOUN eurjchem-112 25 2 : : PUNCT eurjchem-112 25 3     SPACE eurjchem-112 25 4 m m PROPN eurjchem-112 25 5 / / SYM eurjchem-112 25 6 z z NOUN eurjchem-112 25 7     SPACE eurjchem-112 25 8 = = NOUN eurjchem-112 25 9     SPACE eurjchem-112 25 10 331 331 NUM eurjchem-112 25 11     SPACE eurjchem-112 25 12 ( ( PUNCT eurjchem-112 25 13 m+ m+ NUM eurjchem-112 25 14 ) ) PUNCT eurjchem-112 25 15 . . PUNCT eurjchem-112 25 16     SPACE eurjchem-112 26 1 5b 5b NUM eurjchem-112 26 2 : : PUNCT eurjchem-112 26 3     SPACE eurjchem-112 26 4 m.p m.p PROPN eurjchem-112 26 5 . . PROPN eurjchem-112 26 6 : : PUNCT eurjchem-112 26 7     SPACE eurjchem-112 26 8 207 207 NUM eurjchem-112 26 9     SPACE eurjchem-112 26 10 ºc ºc PROPN eurjchem-112 26 11     SPACE eurjchem-112 26 12 ( ( PUNCT eurjchem-112 26 13 lit light VERB eurjchem-112 26 14 . . PUNCT eurjchem-112 26 15     SPACE eurjchem-112 27 1 203‐207 203‐207 NOUN eurjchem-112 27 2     SPACE eurjchem-112 27 3 [ [ X eurjchem-112 27 4 21 21 NUM eurjchem-112 27 5 ] ] PUNCT eurjchem-112 27 6 ) ) PUNCT eurjchem-112 27 7 . . PUNCT eurjchem-112 27 8     SPACE eurjchem-112 28 1 ir ir VERB eurjchem-112 28 2     SPACE eurjchem-112 28 3 ( ( PUNCT eurjchem-112 28 4 kbr kbr PROPN eurjchem-112 28 5 ) ) PUNCT eurjchem-112 28 6     SPACE eurjchem-112 28 7 ( ( PUNCT eurjchem-112 28 8 νmax νmax PROPN eurjchem-112 28 9 , , PUNCT eurjchem-112 28 10     SPACE eurjchem-112 28 11 cm−1 cm−1 NOUN eurjchem-112 28 12 ): ): PUNCT eurjchem-112 28 13     SPACE eurjchem-112 28 14 3467 3467 NUM eurjchem-112 28 15 , , PUNCT eurjchem-112 28 16     SPACE eurjchem-112 28 17 3340 3340 NUM eurjchem-112 28 18 , , PUNCT eurjchem-112 28 19     SPACE eurjchem-112 28 20 2225 2225 NUM eurjchem-112 28 21 . . PUNCT eurjchem-112 28 22     SPACE eurjchem-112 28 23 1h 1h NUM eurjchem-112 28 24     SPACE eurjchem-112 28 25 nmr nmr NOUN eurjchem-112 28 26     SPACE eurjchem-112 28 27 ( ( PUNCT eurjchem-112 28 28 cdcl3 cdcl3 PROPN eurjchem-112 28 29 , , PUNCT eurjchem-112 28 30     SPACE eurjchem-112 28 31 300 300 NUM eurjchem-112 28 32     SPACE eurjchem-112 28 33 mhz mhz NOUN eurjchem-112 28 34 ) ) PUNCT eurjchem-112 28 35     SPACE eurjchem-112 28 36 δh δh NOUN eurjchem-112 28 37     SPACE eurjchem-112 28 38 ( ( PUNCT eurjchem-112 28 39 ppm ppm PROPN eurjchem-112 28 40 ): ): PUNCT eurjchem-112 28 41     SPACE eurjchem-112 28 42 3.75 3.75 NUM eurjchem-112 28 43     SPACE eurjchem-112 28 44 ( ( PUNCT eurjchem-112 28 45 s s PROPN eurjchem-112 28 46 , , PUNCT eurjchem-112 28 47     SPACE eurjchem-112 28 48 3h 3h NUM eurjchem-112 28 49 , , PUNCT eurjchem-112 28 50     SPACE eurjchem-112 28 51 3‐och3 3‐och3 NUM eurjchem-112 28 52 ) ) PUNCT eurjchem-112 28 53 , , PUNCT eurjchem-112 28 54     SPACE eurjchem-112 28 55 3.89 3.89 NUM eurjchem-112 28 56     SPACE eurjchem-112 28 57 ( ( PUNCT eurjchem-112 28 58 s s PROPN eurjchem-112 28 59 , , PUNCT eurjchem-112 28 60     SPACE eurjchem-112 28 61 3h 3h NUM eurjchem-112 28 62 , , PUNCT eurjchem-112 28 63     SPACE eurjchem-112 28 64 4‐och3 4‐och3 NUM eurjchem-112 28 65 ) ) PUNCT eurjchem-112 28 66 , , PUNCT eurjchem-112 28 67     SPACE eurjchem-112 28 68 7.18–7.68 7.18–7.68 NUM eurjchem-112 28 69     SPACE eurjchem-112 28 70 ( ( PUNCT eurjchem-112 28 71 m m PROPN eurjchem-112 28 72 , , PUNCT eurjchem-112 28 73     SPACE eurjchem-112 28 74 8h 8h NUM eurjchem-112 28 75 , , PUNCT eurjchem-112 28 76     SPACE eurjchem-112 28 77 aromatic aromatic NOUN eurjchem-112 28 78 ) ) PUNCT eurjchem-112 28 79 , , PUNCT eurjchem-112 28 80     SPACE eurjchem-112 28 81 10.51 10.51 NUM eurjchem-112 28 82     SPACE eurjchem-112 28 83 ( ( PUNCT eurjchem-112 28 84 brs br VERB eurjchem-112 28 85 , , PUNCT eurjchem-112 28 86     SPACE eurjchem-112 28 87 1h 1h NUM eurjchem-112 28 88 , , PUNCT eurjchem-112 28 89     SPACE eurjchem-112 28 90 nh nh PROPN eurjchem-112 28 91 ) ) PUNCT eurjchem-112 28 92 , , PUNCT eurjchem-112 28 93     SPACE eurjchem-112 28 94 10.62 10.62 NUM eurjchem-112 28 95     SPACE eurjchem-112 28 96 ( ( PUNCT eurjchem-112 28 97 brs br VERB eurjchem-112 28 98 , , PUNCT eurjchem-112 28 99     SPACE eurjchem-112 28 100 1h 1h NUM eurjchem-112 28 101 , , PUNCT eurjchem-112 28 102     SPACE eurjchem-112 28 103 nh nh PROPN eurjchem-112 28 104 ) ) PUNCT eurjchem-112 28 105 . . PUNCT eurjchem-112 28 106     SPACE eurjchem-112 29 1 ms ms NOUN eurjchem-112 29 2 : : PUNCT eurjchem-112 29 3     SPACE eurjchem-112 29 4 m m PROPN eurjchem-112 29 5 / / SYM eurjchem-112 29 6 z z NOUN eurjchem-112 29 7     SPACE eurjchem-112 29 8 = = NOUN eurjchem-112 29 9     SPACE eurjchem-112 29 10 365 365 NUM eurjchem-112 29 11     SPACE eurjchem-112 29 12 ( ( PUNCT eurjchem-112 29 13 m+ m+ NUM eurjchem-112 29 14 ) ) PUNCT eurjchem-112 29 15 . . PUNCT eurjchem-112 29 16     SPACE eurjchem-112 30 1 5c 5c NOUN eurjchem-112 30 2 : : PUNCT eurjchem-112 30 3     SPACE eurjchem-112 30 4 m.p m.p PROPN eurjchem-112 30 5 . . PROPN eurjchem-112 30 6 : : PUNCT eurjchem-112 30 7     SPACE eurjchem-112 30 8 202 202 NUM eurjchem-112 30 9     SPACE eurjchem-112 30 10 ºc ºc PROPN eurjchem-112 30 11     SPACE eurjchem-112 30 12 ( ( PUNCT eurjchem-112 30 13 lit light VERB eurjchem-112 30 14 . . PUNCT eurjchem-112 30 15     SPACE eurjchem-112 31 1 205‐207 205‐207 PROPN eurjchem-112 31 2     SPACE eurjchem-112 32 1 [ [ X eurjchem-112 32 2 21 21 NUM eurjchem-112 32 3 ] ] PUNCT eurjchem-112 32 4 ) ) PUNCT eurjchem-112 32 5 . . PUNCT eurjchem-112 32 6     SPACE eurjchem-112 33 1 ir ir VERB eurjchem-112 33 2     SPACE eurjchem-112 33 3 ( ( PUNCT eurjchem-112 33 4 kbr kbr PROPN eurjchem-112 33 5 ) ) PUNCT eurjchem-112 33 6     SPACE eurjchem-112 33 7 ( ( PUNCT eurjchem-112 33 8 νmax νmax PROPN eurjchem-112 33 9 , , PUNCT eurjchem-112 33 10     SPACE eurjchem-112 33 11 cm−1 cm−1 NOUN eurjchem-112 33 12 ): ): PUNCT eurjchem-112 33 13     SPACE eurjchem-112 33 14 3428 3428 NUM eurjchem-112 33 15 , , PUNCT eurjchem-112 33 16     SPACE eurjchem-112 33 17 3345 3345 NUM eurjchem-112 33 18 , , PUNCT eurjchem-112 33 19     SPACE eurjchem-112 33 20 2246 2246 NUM eurjchem-112 33 21 . . PUNCT eurjchem-112 33 22     SPACE eurjchem-112 33 23 1h 1h NUM eurjchem-112 33 24     SPACE eurjchem-112 33 25 nmr nmr NOUN eurjchem-112 33 26     SPACE eurjchem-112 33 27 ( ( PUNCT eurjchem-112 33 28 cdcl3 cdcl3 PROPN eurjchem-112 33 29 , , PUNCT eurjchem-112 33 30     SPACE eurjchem-112 33 31 300 300 NUM eurjchem-112 33 32     SPACE eurjchem-112 33 33 mhz mhz NOUN eurjchem-112 33 34 ) ) PUNCT eurjchem-112 33 35     SPACE eurjchem-112 33 36 δh δh NOUN eurjchem-112 33 37     SPACE eurjchem-112 33 38 ( ( PUNCT eurjchem-112 33 39 ppm ppm PROPN eurjchem-112 33 40 ): ): PUNCT eurjchem-112 33 41     SPACE eurjchem-112 33 42 3.85 3.85 NUM eurjchem-112 33 43     SPACE eurjchem-112 33 44 ( ( PUNCT eurjchem-112 33 45 s s PROPN eurjchem-112 33 46 , , PUNCT eurjchem-112 33 47     SPACE eurjchem-112 33 48 3h 3h NUM eurjchem-112 33 49 , , PUNCT eurjchem-112 33 50     SPACE eurjchem-112 33 51 3‐och3 3‐och3 NUM eurjchem-112 33 52 ) ) PUNCT eurjchem-112 33 53 , , PUNCT eurjchem-112 33 54     SPACE eurjchem-112 33 55 3.91 3.91 NUM eurjchem-112 33 56     SPACE eurjchem-112 33 57 ( ( PUNCT eurjchem-112 33 58 s s PROPN eurjchem-112 33 59 , , PUNCT eurjchem-112 33 60     SPACE eurjchem-112 33 61 3h 3h NUM eurjchem-112 33 62 , , PUNCT eurjchem-112 33 63     SPACE eurjchem-112 33 64 4‐och3 4‐och3 NUM eurjchem-112 33 65 ) ) PUNCT eurjchem-112 33 66 , , PUNCT eurjchem-112 33 67     SPACE eurjchem-112 33 68 7.12–7.58 7.12–7.58 NUM eurjchem-112 33 69     SPACE eurjchem-112 33 70 ( ( PUNCT eurjchem-112 33 71 m m PROPN eurjchem-112 33 72 , , PUNCT eurjchem-112 33 73     SPACE eurjchem-112 33 74 8h 8h NUM eurjchem-112 33 75 , , PUNCT eurjchem-112 33 76     SPACE eurjchem-112 33 77 aromatic aromatic NOUN eurjchem-112 33 78 ) ) PUNCT eurjchem-112 33 79 , , PUNCT eurjchem-112 33 80     SPACE eurjchem-112 33 81 9.86 9.86 NUM eurjchem-112 33 82     SPACE eurjchem-112 33 83 ( ( PUNCT eurjchem-112 33 84 brs br VERB eurjchem-112 33 85 , , PUNCT eurjchem-112 33 86     SPACE eurjchem-112 33 87 1h 1h NUM eurjchem-112 33 88 , , PUNCT eurjchem-112 33 89     SPACE eurjchem-112 33 90 nh nh PROPN eurjchem-112 33 91 ) ) PUNCT eurjchem-112 33 92 , , PUNCT eurjchem-112 33 93     SPACE eurjchem-112 33 94 9.98 9.98 NUM eurjchem-112 33 95     SPACE eurjchem-112 33 96 ( ( PUNCT eurjchem-112 33 97 1h 1h NUM eurjchem-112 33 98 , , PUNCT eurjchem-112 33 99     SPACE eurjchem-112 33 100 oh oh INTJ eurjchem-112 33 101 ) ) PUNCT eurjchem-112 33 102 , , PUNCT eurjchem-112 33 103     SPACE eurjchem-112 33 104 10.65 10.65 NUM eurjchem-112 33 105     SPACE eurjchem-112 33 106 ( ( PUNCT eurjchem-112 33 107 brs br VERB eurjchem-112 33 108 , , PUNCT eurjchem-112 33 109     SPACE eurjchem-112 33 110 1h 1h NUM eurjchem-112 33 111 , , PUNCT eurjchem-112 33 112     SPACE eurjchem-112 33 113 nh nh PROPN eurjchem-112 33 114 ) ) PUNCT eurjchem-112 33 115 . . PUNCT eurjchem-112 33 116     SPACE eurjchem-112 34 1 ms ms NOUN eurjchem-112 34 2 : : PUNCT eurjchem-112 34 3     SPACE eurjchem-112 34 4 m m PROPN eurjchem-112 34 5 / / SYM eurjchem-112 34 6 z z NOUN eurjchem-112 34 7     SPACE eurjchem-112 34 8 = = VERB eurjchem-112 34 9     SPACE eurjchem-112 34 10 347 347 NUM eurjchem-112 34 11     SPACE eurjchem-112 34 12 ( ( PUNCT eurjchem-112 34 13 m+ m+ NUM eurjchem-112 34 14 ) ) PUNCT eurjchem-112 34 15 . . PUNCT eurjchem-112 34 16     SPACE eurjchem-112 35 1 5d 5d NUM eurjchem-112 35 2 : : PUNCT eurjchem-112 35 3     SPACE eurjchem-112 35 4 m.p m.p PROPN eurjchem-112 35 5 . . PROPN eurjchem-112 35 6 : : PUNCT eurjchem-112 35 7     SPACE eurjchem-112 35 8 167 167 NUM eurjchem-112 35 9     SPACE eurjchem-112 35 10 ºc ºc NOUN eurjchem-112 35 11     SPACE eurjchem-112 35 12 ( ( PUNCT eurjchem-112 35 13 lit light VERB eurjchem-112 35 14 . . PUNCT eurjchem-112 35 15     SPACE eurjchem-112 36 1 165‐167 165‐167 NUM eurjchem-112 36 2     SPACE eurjchem-112 37 1 [ [ X eurjchem-112 37 2 21 21 NUM eurjchem-112 37 3 ] ] PUNCT eurjchem-112 37 4 ) ) PUNCT eurjchem-112 37 5 . . PUNCT eurjchem-112 37 6     SPACE eurjchem-112 38 1 ir ir VERB eurjchem-112 38 2     SPACE eurjchem-112 38 3 ( ( PUNCT eurjchem-112 38 4 kbr kbr PROPN eurjchem-112 38 5 ) ) PUNCT eurjchem-112 38 6     SPACE eurjchem-112 38 7 ( ( PUNCT eurjchem-112 38 8 νmax νmax PROPN eurjchem-112 38 9 , , PUNCT eurjchem-112 38 10     SPACE eurjchem-112 38 11 cm−1 cm−1 NOUN eurjchem-112 38 12 ): ): PUNCT eurjchem-112 38 13     SPACE eurjchem-112 38 14 3429 3429 NUM eurjchem-112 38 15 , , PUNCT eurjchem-112 38 16     SPACE eurjchem-112 38 17 3365 3365 NUM eurjchem-112 38 18 , , PUNCT eurjchem-112 38 19     SPACE eurjchem-112 38 20 2216 2216 NUM eurjchem-112 38 21 . . PUNCT eurjchem-112 38 22     SPACE eurjchem-112 38 23 1h 1h NUM eurjchem-112 38 24     SPACE eurjchem-112 38 25 nmr nmr NOUN eurjchem-112 38 26     SPACE eurjchem-112 38 27 ( ( PUNCT eurjchem-112 38 28 cdcl3 cdcl3 PROPN eurjchem-112 38 29 , , PUNCT eurjchem-112 38 30     SPACE eurjchem-112 38 31 300 300 NUM eurjchem-112 38 32     SPACE eurjchem-112 38 33 mhz mhz NOUN eurjchem-112 38 34 ) ) PUNCT eurjchem-112 38 35     SPACE eurjchem-112 38 36 δh δh NOUN eurjchem-112 38 37     SPACE eurjchem-112 38 38 ( ( PUNCT eurjchem-112 38 39 ppm ppm PROPN eurjchem-112 38 40 ): ): PUNCT eurjchem-112 38 41     SPACE eurjchem-112 38 42 3.61 3.61 NUM eurjchem-112 38 43     SPACE eurjchem-112 38 44 ( ( PUNCT eurjchem-112 38 45 s s PROPN eurjchem-112 38 46 , , PUNCT eurjchem-112 38 47     SPACE eurjchem-112 38 48 3h 3h NUM eurjchem-112 38 49 , , PUNCT eurjchem-112 38 50     SPACE eurjchem-112 38 51 3‐och3 3‐och3 NUM eurjchem-112 38 52 ) ) PUNCT eurjchem-112 38 53 , , PUNCT eurjchem-112 38 54     SPACE eurjchem-112 38 55 3.94 3.94 NUM eurjchem-112 38 56     SPACE eurjchem-112 38 57 ( ( PUNCT eurjchem-112 38 58 s s PROPN eurjchem-112 38 59 , , PUNCT eurjchem-112 38 60     SPACE eurjchem-112 38 61 3h 3h NUM eurjchem-112 38 62 , , PUNCT eurjchem-112 38 63     SPACE eurjchem-112 38 64 4‐och3 4‐och3 NUM eurjchem-112 38 65 ) ) PUNCT eurjchem-112 38 66 , , PUNCT eurjchem-112 38 67     SPACE eurjchem-112 38 68 3.96 3.96 NUM eurjchem-112 38 69     SPACE eurjchem-112 38 70 ( ( PUNCT eurjchem-112 38 71 s s PROPN eurjchem-112 38 72 , , PUNCT eurjchem-112 38 73     SPACE eurjchem-112 38 74 3h 3h NUM eurjchem-112 38 75 ) ) PUNCT eurjchem-112 38 76 , , PUNCT eurjchem-112 38 77     SPACE eurjchem-112 38 78 7.32–7.88 7.32–7.88 NUM eurjchem-112 38 79     SPACE eurjchem-112 38 80 ( ( PUNCT eurjchem-112 38 81 m m PROPN eurjchem-112 38 82 , , PUNCT eurjchem-112 38 83     SPACE eurjchem-112 38 84 8h 8h NUM eurjchem-112 38 85 , , PUNCT eurjchem-112 38 86     SPACE eurjchem-112 38 87 aromatic aromatic NOUN eurjchem-112 38 88 ) ) PUNCT eurjchem-112 38 89 , , PUNCT eurjchem-112 38 90     SPACE eurjchem-112 38 91 10.51 10.51 NUM eurjchem-112 38 92     SPACE eurjchem-112 38 93 ( ( PUNCT eurjchem-112 38 94 brs br VERB eurjchem-112 38 95 , , PUNCT eurjchem-112 38 96     SPACE eurjchem-112 38 97 1h 1h NUM eurjchem-112 38 98 , , PUNCT eurjchem-112 38 99     SPACE eurjchem-112 38 100 nh nh PROPN eurjchem-112 38 101 ) ) PUNCT eurjchem-112 38 102 , , PUNCT eurjchem-112 38 103     SPACE eurjchem-112 38 104 10.62 10.62 NUM eurjchem-112 38 105     SPACE eurjchem-112 38 106 ( ( PUNCT eurjchem-112 38 107 brs br VERB eurjchem-112 38 108 , , PUNCT eurjchem-112 38 109     SPACE eurjchem-112 38 110 1h 1h NUM eurjchem-112 38 111 , , PUNCT eurjchem-112 38 112     SPACE eurjchem-112 38 113 nh nh PROPN eurjchem-112 38 114 ) ) PUNCT eurjchem-112 38 115 . . PUNCT eurjchem-112 38 116     SPACE eurjchem-112 39 1 ms ms NOUN eurjchem-112 39 2 : : PUNCT eurjchem-112 39 3     SPACE eurjchem-112 39 4 m m PROPN eurjchem-112 39 5 / / SYM eurjchem-112 39 6 z z NOUN eurjchem-112 39 7     SPACE eurjchem-112 39 8 = = NOUN eurjchem-112 39 9     SPACE eurjchem-112 39 10 361 361 NUM eurjchem-112 39 11     SPACE eurjchem-112 39 12 ( ( PUNCT eurjchem-112 39 13 m+ m+ NUM eurjchem-112 39 14 ) ) PUNCT eurjchem-112 39 15 . . PUNCT eurjchem-112 39 16     SPACE eurjchem-112 40 1 5e 5e NOUN eurjchem-112 40 2 : : PUNCT eurjchem-112 40 3     SPACE eurjchem-112 40 4 m.p m.p PROPN eurjchem-112 40 5 . . PROPN eurjchem-112 40 6 : : PUNCT eurjchem-112 40 7     SPACE eurjchem-112 40 8 194 194 NUM eurjchem-112 40 9     SPACE eurjchem-112 40 10 ºc ºc PROPN eurjchem-112 40 11     SPACE eurjchem-112 40 12 ( ( PUNCT eurjchem-112 40 13 lit light VERB eurjchem-112 40 14 . . PUNCT eurjchem-112 40 15     SPACE eurjchem-112 41 1 190‐192 190‐192 NUM eurjchem-112 41 2     SPACE eurjchem-112 42 1 [ [ X eurjchem-112 42 2 21 21 NUM eurjchem-112 42 3 ] ] PUNCT eurjchem-112 42 4 ) ) PUNCT eurjchem-112 42 5 . . PUNCT eurjchem-112 42 6     SPACE eurjchem-112 43 1 ir ir VERB eurjchem-112 43 2     SPACE eurjchem-112 43 3 ( ( PUNCT eurjchem-112 43 4 kbr kbr PROPN eurjchem-112 43 5 ) ) PUNCT eurjchem-112 43 6     SPACE eurjchem-112 43 7 ( ( PUNCT eurjchem-112 43 8 νmax νmax PROPN eurjchem-112 43 9 , , PUNCT eurjchem-112 43 10     SPACE eurjchem-112 43 11 cm−1 cm−1 NOUN eurjchem-112 43 12 ): ): PUNCT eurjchem-112 43 13     SPACE eurjchem-112 43 14 3461 3461 NUM eurjchem-112 43 15 , , PUNCT eurjchem-112 43 16     SPACE eurjchem-112 43 17 3310 3310 NUM eurjchem-112 43 18 , , PUNCT eurjchem-112 43 19     SPACE eurjchem-112 43 20 2220 2220 NUM eurjchem-112 43 21 . . PUNCT eurjchem-112 43 22     SPACE eurjchem-112 43 23 1h 1h NUM eurjchem-112 43 24     SPACE eurjchem-112 43 25 nmr nmr NOUN eurjchem-112 43 26     SPACE eurjchem-112 43 27 ( ( PUNCT eurjchem-112 43 28 cdcl3 cdcl3 PROPN eurjchem-112 43 29 , , PUNCT eurjchem-112 43 30     SPACE eurjchem-112 43 31 300 300 NUM eurjchem-112 43 32     SPACE eurjchem-112 43 33 mhz mhz NOUN eurjchem-112 43 34 ) ) PUNCT eurjchem-112 43 35     SPACE eurjchem-112 43 36 δh δh NOUN eurjchem-112 43 37     SPACE eurjchem-112 43 38 ( ( PUNCT eurjchem-112 43 39 ppm ppm PROPN eurjchem-112 43 40 ): ): PUNCT eurjchem-112 43 41     SPACE eurjchem-112 43 42 2.96 2.96 NUM eurjchem-112 43 43     SPACE eurjchem-112 43 44 ( ( PUNCT eurjchem-112 43 45 s s PROPN eurjchem-112 43 46 , , PUNCT eurjchem-112 43 47     SPACE eurjchem-112 43 48 3h 3h NUM eurjchem-112 43 49 ) ) PUNCT eurjchem-112 43 50 , , PUNCT eurjchem-112 43 51     SPACE eurjchem-112 43 52 3.82 3.82 NUM eurjchem-112 43 53     SPACE eurjchem-112 43 54 ( ( PUNCT eurjchem-112 43 55 s s PROPN eurjchem-112 43 56 , , PUNCT eurjchem-112 43 57     SPACE eurjchem-112 43 58 3h 3h NUM eurjchem-112 43 59 , , PUNCT eurjchem-112 43 60     SPACE eurjchem-112 43 61 3‐och3 3‐och3 NUM eurjchem-112 43 62 ) ) PUNCT eurjchem-112 43 63 , , PUNCT eurjchem-112 43 64     SPACE eurjchem-112 43 65 3.93 3.93 NUM eurjchem-112 43 66     SPACE eurjchem-112 43 67 ( ( PUNCT eurjchem-112 43 68 s s PROPN eurjchem-112 43 69 , , PUNCT eurjchem-112 43 70     SPACE eurjchem-112 43 71 3h 3h NUM eurjchem-112 43 72 , , PUNCT eurjchem-112 43 73     SPACE eurjchem-112 43 74 4‐och3 4‐och3 NUM eurjchem-112 43 75 ) ) PUNCT eurjchem-112 43 76 , , PUNCT eurjchem-112 43 77     SPACE eurjchem-112 43 78 7.35–7.63 7.35–7.63 NOUN eurjchem-112 43 79     SPACE eurjchem-112 43 80 ( ( PUNCT eurjchem-112 43 81 m m PROPN eurjchem-112 43 82 , , PUNCT eurjchem-112 43 83     SPACE eurjchem-112 43 84 4h 4h NOUN eurjchem-112 43 85 , , PUNCT eurjchem-112 43 86     SPACE eurjchem-112 43 87 aromatic aromatic NOUN eurjchem-112 43 88 ) ) PUNCT eurjchem-112 43 89 , , PUNCT eurjchem-112 43 90     SPACE eurjchem-112 43 91 10.51 10.51 NUM eurjchem-112 43 92     SPACE eurjchem-112 43 93 ( ( PUNCT eurjchem-112 43 94 brs br VERB eurjchem-112 43 95 , , PUNCT eurjchem-112 43 96     SPACE eurjchem-112 43 97 1h 1h NUM eurjchem-112 43 98 , , PUNCT eurjchem-112 43 99     SPACE eurjchem-112 43 100 nh nh PROPN eurjchem-112 43 101 ) ) PUNCT eurjchem-112 43 102 , , PUNCT eurjchem-112 43 103     SPACE eurjchem-112 43 104 10.62 10.62 NUM eurjchem-112 43 105     SPACE eurjchem-112 43 106 ( ( PUNCT eurjchem-112 43 107 brs br VERB eurjchem-112 43 108 , , PUNCT eurjchem-112 43 109     SPACE eurjchem-112 43 110 1h 1h NUM eurjchem-112 43 111 , , PUNCT eurjchem-112 43 112     SPACE eurjchem-112 43 113 nh nh PROPN eurjchem-112 43 114 ) ) PUNCT eurjchem-112 43 115 . . PUNCT eurjchem-112 43 116     SPACE eurjchem-112 44 1 ms ms NOUN eurjchem-112 44 2 : : PUNCT eurjchem-112 44 3     SPACE eurjchem-112 44 4 m m PROPN eurjchem-112 44 5 / / SYM eurjchem-112 44 6 z z NOUN eurjchem-112 44 7     SPACE eurjchem-112 44 8 = = NOUN eurjchem-112 44 9     SPACE eurjchem-112 44 10 269 269 NUM eurjchem-112 44 11     SPACE eurjchem-112 44 12 ( ( PUNCT eurjchem-112 44 13 m+ m+ NUM eurjchem-112 44 14 ) ) PUNCT eurjchem-112 44 15 . . PUNCT eurjchem-112 44 16     SPACE eurjchem-112 45 1 6a 6a NOUN eurjchem-112 45 2 : : PUNCT eurjchem-112 45 3     SPACE eurjchem-112 45 4 m.p m.p PROPN eurjchem-112 45 5 . . PROPN eurjchem-112 45 6 : : PUNCT eurjchem-112 45 7     SPACE eurjchem-112 45 8 285 285 NUM eurjchem-112 45 9     SPACE eurjchem-112 45 10 ºc ºc PROPN eurjchem-112 45 11     SPACE eurjchem-112 45 12 ( ( PUNCT eurjchem-112 45 13 lit light VERB eurjchem-112 45 14 . . PUNCT eurjchem-112 45 15     SPACE eurjchem-112 46 1 287‐289 287‐289 NUM eurjchem-112 46 2     SPACE eurjchem-112 47 1 [ [ X eurjchem-112 47 2 21 21 NUM eurjchem-112 47 3 ] ] PUNCT eurjchem-112 47 4 ) ) PUNCT eurjchem-112 47 5 . . PUNCT eurjchem-112 47 6     SPACE eurjchem-112 48 1 ir ir VERB eurjchem-112 48 2     SPACE eurjchem-112 48 3 ( ( PUNCT eurjchem-112 48 4 kbr kbr PROPN eurjchem-112 48 5 ) ) PUNCT eurjchem-112 48 6     SPACE eurjchem-112 48 7 ( ( PUNCT eurjchem-112 48 8 νmax νmax PROPN eurjchem-112 48 9 , , PUNCT eurjchem-112 48 10     SPACE eurjchem-112 48 11 cm−1 cm−1 NOUN eurjchem-112 48 12 ): ): PUNCT eurjchem-112 48 13     SPACE eurjchem-112 48 14 3330 3330 NUM eurjchem-112 48 15 , , PUNCT eurjchem-112 48 16     SPACE eurjchem-112 48 17 2228 2228 NUM eurjchem-112 48 18 , , PUNCT eurjchem-112 48 19     SPACE eurjchem-112 48 20 1641 1641 NUM eurjchem-112 48 21 . . PUNCT eurjchem-112 48 22     SPACE eurjchem-112 48 23 1h 1h NUM eurjchem-112 48 24     SPACE eurjchem-112 48 25 nmr nmr NOUN eurjchem-112 48 26     SPACE eurjchem-112 48 27 ( ( PUNCT eurjchem-112 48 28 cdcl3 cdcl3 PROPN eurjchem-112 48 29 , , PUNCT eurjchem-112 48 30     SPACE eurjchem-112 48 31 300 300 NUM eurjchem-112 48 32     SPACE eurjchem-112 48 33 mhz mhz NOUN eurjchem-112 48 34 ) ) PUNCT eurjchem-112 48 35     SPACE eurjchem-112 48 36 δh δh NOUN eurjchem-112 48 37     SPACE eurjchem-112 48 38 ( ( PUNCT eurjchem-112 48 39 ppm ppm PROPN eurjchem-112 48 40 ): ): PUNCT eurjchem-112 48 41     SPACE eurjchem-112 48 42 3.89 3.89 NUM eurjchem-112 48 43     SPACE eurjchem-112 48 44 ( ( PUNCT eurjchem-112 48 45 s s PROPN eurjchem-112 48 46 , , PUNCT eurjchem-112 48 47     SPACE eurjchem-112 48 48 3h 3h NUM eurjchem-112 48 49 , , PUNCT eurjchem-112 48 50     SPACE eurjchem-112 48 51 3‐och3 3‐och3 NUM eurjchem-112 48 52 ) ) PUNCT eurjchem-112 48 53 , , PUNCT eurjchem-112 48 54     SPACE eurjchem-112 48 55 4.01 4.01 NUM eurjchem-112 48 56     SPACE eurjchem-112 48 57 ( ( PUNCT eurjchem-112 48 58 s s PROPN eurjchem-112 48 59 , , PUNCT eurjchem-112 48 60     SPACE eurjchem-112 48 61 3h 3h NUM eurjchem-112 48 62 , , PUNCT eurjchem-112 48 63     SPACE eurjchem-112 48 64 4‐och3 4‐och3 NUM eurjchem-112 48 65 ) ) PUNCT eurjchem-112 48 66 , , PUNCT eurjchem-112 48 67     SPACE eurjchem-112 48 68 7.09–7.52 7.09–7.52 NUM eurjchem-112 48 69     SPACE eurjchem-112 48 70 ( ( PUNCT eurjchem-112 48 71 m m PROPN eurjchem-112 48 72 , , PUNCT eurjchem-112 48 73     SPACE eurjchem-112 48 74 9h 9h NOUN eurjchem-112 48 75 , , PUNCT eurjchem-112 48 76     SPACE eurjchem-112 48 77 aromatic aromatic NOUN eurjchem-112 48 78 ) ) PUNCT eurjchem-112 48 79 , , PUNCT eurjchem-112 48 80     SPACE eurjchem-112 48 81 12.51 12.51 NUM eurjchem-112 48 82     SPACE eurjchem-112 48 83 ( ( PUNCT eurjchem-112 48 84 brs br VERB eurjchem-112 48 85 , , PUNCT eurjchem-112 48 86     SPACE eurjchem-112 48 87 1h 1h NUM eurjchem-112 48 88 , , PUNCT eurjchem-112 48 89     SPACE eurjchem-112 48 90 nh nh PROPN eurjchem-112 48 91 ) ) PUNCT eurjchem-112 48 92 . . PUNCT eurjchem-112 48 93     SPACE eurjchem-112 49 1 ms ms NOUN eurjchem-112 49 2 : : PUNCT eurjchem-112 49 3     SPACE eurjchem-112 49 4 m m PROPN eurjchem-112 49 5 / / SYM eurjchem-112 49 6 z z NOUN eurjchem-112 49 7     SPACE eurjchem-112 49 8 = = NOUN eurjchem-112 49 9     SPACE eurjchem-112 49 10 332 332 NUM eurjchem-112 49 11     SPACE eurjchem-112 49 12 ( ( PUNCT eurjchem-112 49 13 m+ m+ NUM eurjchem-112 49 14 ) ) PUNCT eurjchem-112 49 15 . . PUNCT eurjchem-112 49 16     SPACE eurjchem-112 50 1 6b 6b NOUN eurjchem-112 50 2 : : PUNCT eurjchem-112 50 3     SPACE eurjchem-112 50 4 m.p m.p PROPN eurjchem-112 50 5 . . PROPN eurjchem-112 50 6 : : PUNCT eurjchem-112 50 7     SPACE eurjchem-112 50 8 295 295 NUM eurjchem-112 50 9     SPACE eurjchem-112 50 10 ºc ºc NOUN eurjchem-112 50 11     SPACE eurjchem-112 50 12 ( ( PUNCT eurjchem-112 50 13 lit light VERB eurjchem-112 50 14 . . PUNCT eurjchem-112 50 15     SPACE eurjchem-112 51 1 292‐294 292‐294 NOUN eurjchem-112 51 2     SPACE eurjchem-112 51 3 [ [ X eurjchem-112 51 4 21 21 NUM eurjchem-112 51 5 ] ] PUNCT eurjchem-112 51 6 ) ) PUNCT eurjchem-112 51 7 . . PUNCT eurjchem-112 51 8     SPACE eurjchem-112 52 1 ir ir VERB eurjchem-112 52 2     SPACE eurjchem-112 52 3 ( ( PUNCT eurjchem-112 52 4 kbr kbr PROPN eurjchem-112 52 5 ) ) PUNCT eurjchem-112 52 6     SPACE eurjchem-112 52 7 ( ( PUNCT eurjchem-112 52 8 νmax νmax PROPN eurjchem-112 52 9 , , PUNCT eurjchem-112 52 10     SPACE eurjchem-112 52 11 cm−1 cm−1 NOUN eurjchem-112 52 12 ): ): PUNCT eurjchem-112 52 13     SPACE eurjchem-112 52 14 3425 3425 NUM eurjchem-112 52 15 , , PUNCT eurjchem-112 52 16     SPACE eurjchem-112 52 17 2220 2220 NUM eurjchem-112 52 18 , , PUNCT eurjchem-112 52 19     SPACE eurjchem-112 52 20 1638 1638 NUM eurjchem-112 52 21 . . PUNCT eurjchem-112 52 22     SPACE eurjchem-112 52 23 1h 1h NUM eurjchem-112 52 24     SPACE eurjchem-112 52 25 nmr nmr NOUN eurjchem-112 52 26     SPACE eurjchem-112 52 27 ( ( PUNCT eurjchem-112 52 28 cdcl3 cdcl3 PROPN eurjchem-112 52 29 , , PUNCT eurjchem-112 52 30     SPACE eurjchem-112 52 31 300 300 NUM eurjchem-112 52 32     SPACE eurjchem-112 52 33 mhz mhz NOUN eurjchem-112 52 34 ) ) PUNCT eurjchem-112 52 35     SPACE eurjchem-112 52 36 δh δh NOUN eurjchem-112 52 37     SPACE eurjchem-112 52 38 ( ( PUNCT eurjchem-112 52 39 ppm ppm PROPN eurjchem-112 52 40 ): ): PUNCT eurjchem-112 52 41     SPACE eurjchem-112 52 42 3.78 3.78 NUM eurjchem-112 52 43     SPACE eurjchem-112 52 44 ( ( PUNCT eurjchem-112 52 45 s s PROPN eurjchem-112 52 46 , , PUNCT eurjchem-112 52 47     SPACE eurjchem-112 52 48 3h 3h NUM eurjchem-112 52 49 , , PUNCT eurjchem-112 52 50     SPACE eurjchem-112 52 51 3‐och3 3‐och3 NUM eurjchem-112 52 52 ) ) PUNCT eurjchem-112 52 53 , , PUNCT eurjchem-112 52 54     SPACE eurjchem-112 52 55 3.94 3.94 NUM eurjchem-112 52 56     SPACE eurjchem-112 52 57 ( ( PUNCT eurjchem-112 52 58 s s PROPN eurjchem-112 52 59 , , PUNCT eurjchem-112 52 60     SPACE eurjchem-112 52 61 3h 3h NUM eurjchem-112 52 62 , , PUNCT eurjchem-112 52 63     SPACE eurjchem-112 52 64 4‐och3 4‐och3 NUM eurjchem-112 52 65 ) ) PUNCT eurjchem-112 52 66 , , PUNCT eurjchem-112 52 67     SPACE eurjchem-112 52 68 7.11–7.63 7.11–7.63 NUM eurjchem-112 52 69     SPACE eurjchem-112 52 70 ( ( PUNCT eurjchem-112 52 71 m m PROPN eurjchem-112 52 72 , , PUNCT eurjchem-112 52 73     SPACE eurjchem-112 52 74 8h 8h NUM eurjchem-112 52 75 , , PUNCT eurjchem-112 52 76     SPACE eurjchem-112 52 77 aromatic aromatic NOUN eurjchem-112 52 78 ) ) PUNCT eurjchem-112 52 79 , , PUNCT eurjchem-112 52 80     SPACE eurjchem-112 52 81 11.92 11.92 NUM eurjchem-112 52 82     SPACE eurjchem-112 52 83 ( ( PUNCT eurjchem-112 52 84 brs br VERB eurjchem-112 52 85 , , PUNCT eurjchem-112 52 86     SPACE eurjchem-112 52 87 1h 1h NUM eurjchem-112 52 88 , , PUNCT eurjchem-112 52 89     SPACE eurjchem-112 52 90 nh nh PROPN eurjchem-112 52 91 ) ) PUNCT eurjchem-112 52 92 . . PUNCT eurjchem-112 52 93     SPACE eurjchem-112 53 1 ms ms NOUN eurjchem-112 53 2 : : PUNCT eurjchem-112 53 3     SPACE eurjchem-112 53 4 m m PROPN eurjchem-112 53 5 / / SYM eurjchem-112 53 6 z z NOUN eurjchem-112 53 7     SPACE eurjchem-112 53 8 = = NOUN eurjchem-112 53 9     SPACE eurjchem-112 53 10 366 366 NUM eurjchem-112 53 11     SPACE eurjchem-112 53 12 ( ( PUNCT eurjchem-112 53 13 m+ m+ NUM eurjchem-112 53 14 ) ) PUNCT eurjchem-112 53 15 . . PUNCT eurjchem-112 53 16     SPACE eurjchem-112 54 1 6c 6c NUM eurjchem-112 54 2 : : PUNCT eurjchem-112 54 3     SPACE eurjchem-112 54 4 m.p m.p PROPN eurjchem-112 54 5 . . PROPN eurjchem-112 54 6 : : PUNCT eurjchem-112 54 7     SPACE eurjchem-112 54 8 311 311 NUM eurjchem-112 54 9     SPACE eurjchem-112 54 10 ºc ºc PROPN eurjchem-112 54 11     SPACE eurjchem-112 54 12 ( ( PUNCT eurjchem-112 54 13 lit light VERB eurjchem-112 54 14 . . PUNCT eurjchem-112 54 15     SPACE eurjchem-112 54 16 > > X eurjchem-112 55 1 300 300 NUM eurjchem-112 55 2     SPACE eurjchem-112 56 1 [ [ PUNCT eurjchem-112 56 2 21 21 NUM eurjchem-112 56 3 ] ] PUNCT eurjchem-112 56 4 ) ) PUNCT eurjchem-112 56 5 . . PUNCT eurjchem-112 56 6     SPACE eurjchem-112 57 1 ir ir VERB eurjchem-112 57 2     SPACE eurjchem-112 57 3 ( ( PUNCT eurjchem-112 57 4 kbr kbr PROPN eurjchem-112 57 5 ) ) PUNCT eurjchem-112 57 6     SPACE eurjchem-112 57 7 ( ( PUNCT eurjchem-112 57 8 νmax νmax PROPN eurjchem-112 57 9 , , PUNCT eurjchem-112 57 10     SPACE eurjchem-112 57 11 cm−1 cm−1 NOUN eurjchem-112 57 12 ): ): PUNCT eurjchem-112 57 13     SPACE eurjchem-112 57 14 3328 3328 NUM eurjchem-112 57 15 , , PUNCT eurjchem-112 57 16     SPACE eurjchem-112 57 17 2200 2200 NUM eurjchem-112 57 18 , , PUNCT eurjchem-112 57 19     SPACE eurjchem-112 57 20 1658 1658 NUM eurjchem-112 57 21 . . PUNCT eurjchem-112 57 22     SPACE eurjchem-112 57 23 1h 1h NUM eurjchem-112 57 24     SPACE eurjchem-112 57 25 nmr nmr NOUN eurjchem-112 57 26     SPACE eurjchem-112 57 27 ( ( PUNCT eurjchem-112 57 28 cdcl3 cdcl3 PROPN eurjchem-112 57 29 , , PUNCT eurjchem-112 57 30     SPACE eurjchem-112 57 31 300 300 NUM eurjchem-112 57 32     SPACE eurjchem-112 57 33 mhz mhz NOUN eurjchem-112 57 34 ) ) PUNCT eurjchem-112 57 35     SPACE eurjchem-112 57 36 δh δh NOUN eurjchem-112 57 37     SPACE eurjchem-112 57 38 ( ( PUNCT eurjchem-112 57 39 ppm ppm PROPN eurjchem-112 57 40 ): ): PUNCT eurjchem-112 57 41     SPACE eurjchem-112 57 42 3.92 3.92 NUM eurjchem-112 57 43     SPACE eurjchem-112 57 44 ( ( PUNCT eurjchem-112 57 45 s s PROPN eurjchem-112 57 46 , , PUNCT eurjchem-112 57 47     SPACE eurjchem-112 57 48 3h 3h NUM eurjchem-112 57 49 , , PUNCT eurjchem-112 57 50     SPACE eurjchem-112 57 51 3‐ 3‐ NUM eurjchem-112 57 52 och3 och3 ADJ eurjchem-112 57 53 ) ) PUNCT eurjchem-112 57 54 , , PUNCT eurjchem-112 57 55     SPACE eurjchem-112 57 56 4.06 4.06 NUM eurjchem-112 57 57     SPACE eurjchem-112 57 58 ( ( PUNCT eurjchem-112 57 59 s s PROPN eurjchem-112 57 60 , , PUNCT eurjchem-112 57 61     SPACE eurjchem-112 57 62 3h 3h NUM eurjchem-112 57 63 , , PUNCT eurjchem-112 57 64     SPACE eurjchem-112 57 65 4‐och3 4‐och3 NUM eurjchem-112 57 66 ) ) PUNCT eurjchem-112 57 67 , , PUNCT eurjchem-112 57 68     SPACE eurjchem-112 57 69 7.10–7.58 7.10–7.58 NUM eurjchem-112 57 70     SPACE eurjchem-112 57 71 ( ( PUNCT eurjchem-112 57 72 m m PROPN eurjchem-112 57 73 , , PUNCT eurjchem-112 57 74     SPACE eurjchem-112 57 75 8h 8h NUM eurjchem-112 57 76 , , PUNCT eurjchem-112 57 77     SPACE eurjchem-112 57 78 aromatic aromatic NOUN eurjchem-112 57 79 ) ) PUNCT eurjchem-112 57 80 , , PUNCT eurjchem-112 57 81     SPACE eurjchem-112 57 82 11.13 11.13 NUM eurjchem-112 57 83     SPACE eurjchem-112 57 84 ( ( PUNCT eurjchem-112 57 85 1h 1h NUM eurjchem-112 57 86 , , PUNCT eurjchem-112 57 87     SPACE eurjchem-112 57 88 oh oh INTJ eurjchem-112 57 89 ) ) PUNCT eurjchem-112 57 90 , , PUNCT eurjchem-112 57 91     SPACE eurjchem-112 57 92 12.65 12.65 NUM eurjchem-112 57 93     SPACE eurjchem-112 57 94 ( ( PUNCT eurjchem-112 57 95 brs br VERB eurjchem-112 57 96 , , PUNCT eurjchem-112 57 97     SPACE eurjchem-112 57 98 1h 1h NUM eurjchem-112 57 99 , , PUNCT eurjchem-112 57 100     SPACE eurjchem-112 57 101 nh nh PROPN eurjchem-112 57 102 ) ) PUNCT eurjchem-112 57 103 . . PUNCT eurjchem-112 57 104     SPACE eurjchem-112 58 1 ms ms NOUN eurjchem-112 58 2 : : PUNCT eurjchem-112 58 3     SPACE eurjchem-112 58 4 m m PROPN eurjchem-112 58 5 / / SYM eurjchem-112 58 6 z z NOUN eurjchem-112 58 7     SPACE eurjchem-112 58 8 = = NOUN eurjchem-112 58 9     SPACE eurjchem-112 58 10 348 348 NUM eurjchem-112 58 11     SPACE eurjchem-112 58 12 ( ( PUNCT eurjchem-112 58 13 m+ m+ NUM eurjchem-112 58 14 ) ) PUNCT eurjchem-112 58 15 . . PUNCT eurjchem-112 58 16     SPACE eurjchem-112 59 1 6d 6d NUM eurjchem-112 59 2 : : PUNCT eurjchem-112 59 3     SPACE eurjchem-112 59 4 m.p m.p PROPN eurjchem-112 59 5 . . PROPN eurjchem-112 59 6 : : PUNCT eurjchem-112 59 7     SPACE eurjchem-112 59 8 266 266 NUM eurjchem-112 59 9     SPACE eurjchem-112 59 10 ºc ºc NOUN eurjchem-112 59 11     SPACE eurjchem-112 59 12 ( ( PUNCT eurjchem-112 59 13 lit light VERB eurjchem-112 59 14 . . PUNCT eurjchem-112 59 15     SPACE eurjchem-112 60 1 262‐264 262‐264 NOUN eurjchem-112 60 2     SPACE eurjchem-112 61 1 [ [ X eurjchem-112 61 2 21 21 NUM eurjchem-112 61 3 ] ] PUNCT eurjchem-112 61 4 ) ) PUNCT eurjchem-112 61 5 . . PUNCT eurjchem-112 61 6     SPACE eurjchem-112 62 1 ir ir VERB eurjchem-112 62 2     SPACE eurjchem-112 62 3 ( ( PUNCT eurjchem-112 62 4 kbr kbr PROPN eurjchem-112 62 5 ) ) PUNCT eurjchem-112 62 6     SPACE eurjchem-112 62 7 ( ( PUNCT eurjchem-112 62 8 νmax νmax PROPN eurjchem-112 62 9 , , PUNCT eurjchem-112 62 10     SPACE eurjchem-112 62 11 cm−1 cm−1 NOUN eurjchem-112 62 12 ): ): PUNCT eurjchem-112 62 13     SPACE eurjchem-112 62 14 3354 3354 NUM eurjchem-112 62 15 , , PUNCT eurjchem-112 62 16     SPACE eurjchem-112 62 17 2238 2238 NUM eurjchem-112 62 18 , , PUNCT eurjchem-112 62 19     SPACE eurjchem-112 62 20 1642 1642 NUM eurjchem-112 62 21 . . PUNCT eurjchem-112 62 22     SPACE eurjchem-112 62 23 1h 1h NUM eurjchem-112 62 24     SPACE eurjchem-112 62 25 nmr nmr NOUN eurjchem-112 62 26     SPACE eurjchem-112 62 27 ( ( PUNCT eurjchem-112 62 28 cdcl3 cdcl3 PROPN eurjchem-112 62 29 , , PUNCT eurjchem-112 62 30     SPACE eurjchem-112 62 31 300 300 NUM eurjchem-112 62 32     SPACE eurjchem-112 62 33 mhz mhz NOUN eurjchem-112 62 34 ) ) PUNCT eurjchem-112 62 35     SPACE eurjchem-112 62 36 δh δh NOUN eurjchem-112 62 37     SPACE eurjchem-112 62 38 ( ( PUNCT eurjchem-112 62 39 ppm ppm PROPN eurjchem-112 62 40 ): ): PUNCT eurjchem-112 62 41     SPACE eurjchem-112 62 42 3.79 3.79 NUM eurjchem-112 62 43     SPACE eurjchem-112 62 44 ( ( PUNCT eurjchem-112 62 45 s s PROPN eurjchem-112 62 46 , , PUNCT eurjchem-112 62 47     SPACE eurjchem-112 62 48 3h 3h NUM eurjchem-112 62 49 , , PUNCT eurjchem-112 62 50     SPACE eurjchem-112 62 51 3‐och3 3‐och3 NUM eurjchem-112 62 52 ) ) PUNCT eurjchem-112 62 53 , , PUNCT eurjchem-112 62 54     SPACE eurjchem-112 62 55 3.84 3.84 NUM eurjchem-112 62 56     SPACE eurjchem-112 62 57 ( ( PUNCT eurjchem-112 62 58 s s PROPN eurjchem-112 62 59 , , PUNCT eurjchem-112 62 60     SPACE eurjchem-112 62 61 3h 3h NUM eurjchem-112 62 62 , , PUNCT eurjchem-112 62 63     SPACE eurjchem-112 62 64 4‐och3 4‐och3 NUM eurjchem-112 62 65 ) ) PUNCT eurjchem-112 62 66 , , PUNCT eurjchem-112 62 67     SPACE eurjchem-112 62 68 3.96 3.96 NUM eurjchem-112 62 69     SPACE eurjchem-112 62 70 ( ( PUNCT eurjchem-112 62 71 s s PROPN eurjchem-112 62 72 , , PUNCT eurjchem-112 62 73     SPACE eurjchem-112 62 74 3h 3h NUM eurjchem-112 62 75 ) ) PUNCT eurjchem-112 62 76 , , PUNCT eurjchem-112 62 77         SPACE eurjchem-112 62 78 7.22–7.68 7.22–7.68 NUM eurjchem-112 62 79     SPACE eurjchem-112 62 80 ( ( PUNCT eurjchem-112 62 81 m m PROPN eurjchem-112 62 82 , , PUNCT eurjchem-112 62 83     SPACE eurjchem-112 62 84 8h 8h NUM eurjchem-112 62 85 , , PUNCT eurjchem-112 62 86     SPACE eurjchem-112 62 87 aromatic aromatic NOUN eurjchem-112 62 88 ) ) PUNCT eurjchem-112 62 89 , , PUNCT eurjchem-112 62 90     SPACE eurjchem-112 62 91 11.96 11.96 NUM eurjchem-112 62 92     SPACE eurjchem-112 62 93 ( ( PUNCT eurjchem-112 62 94 brs br VERB eurjchem-112 62 95 , , PUNCT eurjchem-112 62 96     SPACE eurjchem-112 62 97 1h 1h NUM eurjchem-112 62 98 , , PUNCT eurjchem-112 62 99     SPACE eurjchem-112 62 100 nh nh PROPN eurjchem-112 62 101 ) ) PUNCT eurjchem-112 62 102 . . PUNCT eurjchem-112 62 103     SPACE eurjchem-112 63 1 ms ms NOUN eurjchem-112 63 2 : : PUNCT eurjchem-112 63 3     SPACE eurjchem-112 63 4 m m PROPN eurjchem-112 63 5 / / SYM eurjchem-112 63 6 z z NOUN eurjchem-112 63 7     SPACE eurjchem-112 63 8 = = NOUN eurjchem-112 63 9     SPACE eurjchem-112 63 10 362 362 NUM eurjchem-112 63 11     SPACE eurjchem-112 63 12 ( ( PUNCT eurjchem-112 63 13 m+ m+ NUM eurjchem-112 63 14 ) ) PUNCT eurjchem-112 63 15 . . PUNCT eurjchem-112 63 16     SPACE eurjchem-112 64 1 6e 6e NOUN eurjchem-112 64 2 : : PUNCT eurjchem-112 64 3     SPACE eurjchem-112 64 4 m.p m.p PROPN eurjchem-112 64 5 . . PROPN eurjchem-112 64 6 : : PUNCT eurjchem-112 64 7     SPACE eurjchem-112 64 8 255 255 NUM eurjchem-112 64 9     SPACE eurjchem-112 64 10 ºc ºc PROPN eurjchem-112 64 11     SPACE eurjchem-112 64 12 ( ( PUNCT eurjchem-112 64 13 lit light VERB eurjchem-112 64 14 . . PUNCT eurjchem-112 64 15     SPACE eurjchem-112 65 1 255‐257 255‐257 NOUN eurjchem-112 65 2     SPACE eurjchem-112 66 1 [ [ X eurjchem-112 66 2 21 21 NUM eurjchem-112 66 3 ] ] PUNCT eurjchem-112 66 4 ) ) PUNCT eurjchem-112 66 5 . . PUNCT eurjchem-112 66 6     SPACE eurjchem-112 67 1 ir ir VERB eurjchem-112 67 2     SPACE eurjchem-112 67 3 ( ( PUNCT eurjchem-112 67 4 kbr kbr PROPN eurjchem-112 67 5 ) ) PUNCT eurjchem-112 67 6     SPACE eurjchem-112 67 7 ( ( PUNCT eurjchem-112 67 8 νmax νmax PROPN eurjchem-112 67 9 , , PUNCT eurjchem-112 67 10     SPACE eurjchem-112 67 11 cm−1 cm−1 NOUN eurjchem-112 67 12 ): ): PUNCT eurjchem-112 67 13     SPACE eurjchem-112 67 14 1670 1670 NUM eurjchem-112 67 15 , , PUNCT eurjchem-112 67 16     SPACE eurjchem-112 67 17 2220 2220 NUM eurjchem-112 67 18 , , PUNCT eurjchem-112 67 19     SPACE eurjchem-112 67 20 3320.1h 3320.1h NUM eurjchem-112 67 21     SPACE eurjchem-112 67 22 nmr nmr NOUN eurjchem-112 67 23     SPACE eurjchem-112 67 24 ( ( PUNCT eurjchem-112 67 25 cdcl3 cdcl3 PROPN eurjchem-112 67 26 , , PUNCT eurjchem-112 67 27     SPACE eurjchem-112 67 28 300 300 NUM eurjchem-112 67 29     SPACE eurjchem-112 67 30 mhz mhz NOUN eurjchem-112 67 31 ) ) PUNCT eurjchem-112 67 32     SPACE eurjchem-112 67 33 δh δh NOUN eurjchem-112 67 34     SPACE eurjchem-112 67 35 ( ( PUNCT eurjchem-112 67 36 ppm ppm PROPN eurjchem-112 67 37 ): ): PUNCT eurjchem-112 67 38     SPACE eurjchem-112 67 39 2.43 2.43 NUM eurjchem-112 67 40     SPACE eurjchem-112 67 41 ( ( PUNCT eurjchem-112 67 42 s s PROPN eurjchem-112 67 43 , , PUNCT eurjchem-112 67 44     SPACE eurjchem-112 67 45 3h 3h NUM eurjchem-112 67 46 , , PUNCT eurjchem-112 67 47     SPACE eurjchem-112 67 48 ch3 ch3 PROPN eurjchem-112 67 49 ) ) PUNCT eurjchem-112 67 50 , , PUNCT eurjchem-112 67 51     SPACE eurjchem-112 67 52 3.75 3.75 NUM eurjchem-112 67 53     SPACE eurjchem-112 67 54 ( ( PUNCT eurjchem-112 67 55 s s PROPN eurjchem-112 67 56 , , PUNCT eurjchem-112 67 57     SPACE eurjchem-112 67 58 3h 3h NUM eurjchem-112 67 59 , , PUNCT eurjchem-112 67 60     SPACE eurjchem-112 67 61 3‐och3 3‐och3 NUM eurjchem-112 67 62 ) ) PUNCT eurjchem-112 67 63 , , PUNCT eurjchem-112 67 64     SPACE eurjchem-112 67 65 3.89 3.89 NUM eurjchem-112 67 66     SPACE eurjchem-112 67 67 ( ( PUNCT eurjchem-112 67 68 s s PROPN eurjchem-112 67 69 , , PUNCT eurjchem-112 67 70     SPACE eurjchem-112 67 71 3h 3h NUM eurjchem-112 67 72 , , PUNCT eurjchem-112 67 73     SPACE eurjchem-112 67 74 4‐och3 4‐och3 NUM eurjchem-112 67 75 ) ) PUNCT eurjchem-112 67 76 , , PUNCT eurjchem-112 67 77     SPACE eurjchem-112 67 78 7.01–7.49 7.01–7.49 NUM eurjchem-112 67 79     SPACE eurjchem-112 67 80 ( ( PUNCT eurjchem-112 67 81 m m PROPN eurjchem-112 67 82 , , PUNCT eurjchem-112 67 83     SPACE eurjchem-112 67 84 4h 4h NOUN eurjchem-112 67 85 , , PUNCT eurjchem-112 67 86     SPACE eurjchem-112 67 87 aromatic aromatic NOUN eurjchem-112 67 88 ) ) PUNCT eurjchem-112 67 89 , , PUNCT eurjchem-112 67 90     SPACE eurjchem-112 67 91 12.05 12.05 NUM eurjchem-112 67 92     SPACE eurjchem-112 67 93 ( ( PUNCT eurjchem-112 67 94 brs br VERB eurjchem-112 67 95 , , PUNCT eurjchem-112 67 96     SPACE eurjchem-112 67 97 1h 1h NUM eurjchem-112 67 98 , , PUNCT eurjchem-112 67 99     SPACE eurjchem-112 67 100 nh nh PROPN eurjchem-112 67 101 ) ) PUNCT eurjchem-112 67 102 . . PUNCT eurjchem-112 67 103     SPACE eurjchem-112 68 1 ms ms NOUN eurjchem-112 68 2 : : PUNCT eurjchem-112 68 3     SPACE eurjchem-112 68 4 m m PROPN eurjchem-112 68 5 / / SYM eurjchem-112 68 6 z z NOUN eurjchem-112 68 7     SPACE eurjchem-112 68 8 = = NOUN eurjchem-112 68 9     SPACE eurjchem-112 68 10 270 270 NUM eurjchem-112 68 11     SPACE eurjchem-112 68 12 ( ( PUNCT eurjchem-112 68 13 m+ m+ NUM eurjchem-112 68 14 ) ) PUNCT eurjchem-112 68 15 . . PUNCT eurjchem-112 68 16         SPACE eurjchem-112 69 1 3 3 X eurjchem-112 69 2 . . PUNCT eurjchem-112 69 3     SPACE eurjchem-112 69 4 results result VERB eurjchem-112 69 5     SPACE eurjchem-112 69 6 and and CCONJ eurjchem-112 69 7     SPACE eurjchem-112 69 8 discussion discussion NOUN eurjchem-112 69 9           SPACE eurjchem-112 69 10 dabco dabco NOUN eurjchem-112 69 11     SPACE eurjchem-112 69 12 has have AUX eurjchem-112 69 13     SPACE eurjchem-112 69 14 been be AUX eurjchem-112 69 15     SPACE eurjchem-112 69 16 widely widely ADV eurjchem-112 69 17     SPACE eurjchem-112 69 18 used use VERB eurjchem-112 69 19     SPACE eurjchem-112 69 20 as as ADP eurjchem-112 69 21     SPACE eurjchem-112 69 22 a a DET eurjchem-112 69 23     SPACE eurjchem-112 69 24 catalyst catalyst NOUN eurjchem-112 69 25     SPACE eurjchem-112 69 26 for for ADP eurjchem-112 69 27     SPACE eurjchem-112 69 28 the the DET eurjchem-112 69 29     SPACE eurjchem-112 69 30 baylis baylis PROPN eurjchem-112 69 31 – – PUNCT eurjchem-112 69 32 hillman hillman NOUN eurjchem-112 69 33     SPACE eurjchem-112 69 34 reactions reaction NOUN eurjchem-112 69 35     SPACE eurjchem-112 70 1 [ [ X eurjchem-112 70 2 9 9 NUM eurjchem-112 70 3 ] ] PUNCT eurjchem-112 70 4 . . PUNCT eurjchem-112 70 5     SPACE eurjchem-112 70 6 it it PRON eurjchem-112 70 7     SPACE eurjchem-112 70 8 has have AUX eurjchem-112 70 9     SPACE eurjchem-112 70 10 also also ADV eurjchem-112 70 11     SPACE eurjchem-112 70 12 been be AUX eurjchem-112 70 13     SPACE eurjchem-112 70 14 reported report VERB eurjchem-112 70 15     SPACE eurjchem-112 70 16 as as ADP eurjchem-112 70 17     SPACE eurjchem-112 70 18 a a DET eurjchem-112 70 19     SPACE eurjchem-112 70 20 catalyst catalyst NOUN eurjchem-112 70 21     SPACE eurjchem-112 70 22 for for ADP eurjchem-112 70 23     SPACE eurjchem-112 70 24 acceleration acceleration NOUN eurjchem-112 70 25     SPACE eurjchem-112 70 26 of of ADP eurjchem-112 70 27     SPACE eurjchem-112 70 28 benzoylation benzoylation NOUN eurjchem-112 70 29     SPACE eurjchem-112 70 30 reactions reaction NOUN eurjchem-112 70 31     SPACE eurjchem-112 71 1 [ [ X eurjchem-112 71 2 10 10 NUM eurjchem-112 71 3 ] ] PUNCT eurjchem-112 71 4 . . PUNCT eurjchem-112 71 5     SPACE eurjchem-112 71 6 dabco dabco PROPN eurjchem-112 71 7     SPACE eurjchem-112 71 8 has have AUX eurjchem-112 71 9     SPACE eurjchem-112 71 10 been be AUX eurjchem-112 71 11     SPACE eurjchem-112 71 12 applied apply VERB eurjchem-112 71 13     SPACE eurjchem-112 71 14 for for ADP eurjchem-112 71 15     SPACE eurjchem-112 71 16 the the DET eurjchem-112 71 17     SPACE eurjchem-112 71 18 synthesis synthesis NOUN eurjchem-112 71 19     SPACE eurjchem-112 71 20 of of ADP eurjchem-112 71 21     SPACE eurjchem-112 71 22 zeolite zeolite NOUN eurjchem-112 71 23     SPACE eurjchem-112 71 24 as as ADP eurjchem-112 71 25     SPACE eurjchem-112 71 26 a a DET eurjchem-112 71 27     SPACE eurjchem-112 71 28 structure structure NOUN eurjchem-112 71 29     SPACE eurjchem-112 71 30 directing direct VERB eurjchem-112 71 31     SPACE eurjchem-112 71 32 agent agent NOUN eurjchem-112 71 33     SPACE eurjchem-112 72 1 [ [ X eurjchem-112 72 2 11 11 NUM eurjchem-112 72 3 ] ] SYM eurjchem-112 72 4     SPACE eurjchem-112 72 5 and and CCONJ eurjchem-112 72 6     SPACE eurjchem-112 72 7 can can AUX eurjchem-112 72 8     SPACE eurjchem-112 72 9 catalyze catalyze VERB eurjchem-112 72 10     SPACE eurjchem-112 72 11 the the DET eurjchem-112 72 12     SPACE eurjchem-112 72 13 self self NOUN eurjchem-112 72 14     SPACE eurjchem-112 72 15 and and CCONJ eurjchem-112 72 16     SPACE eurjchem-112 72 17 cross‐condensation cross‐condensation NOUN eurjchem-112 72 18     SPACE eurjchem-112 72 19 of of ADP eurjchem-112 72 20     SPACE eurjchem-112 72 21 α‐acethylenic α‐acethylenic NUM eurjchem-112 72 22     SPACE eurjchem-112 72 23 ketones ketone NOUN eurjchem-112 72 24     SPACE eurjchem-112 72 25 [ [ X eurjchem-112 72 26 12 12 NUM eurjchem-112 72 27 ] ] PUNCT eurjchem-112 72 28 . . PUNCT eurjchem-112 72 29     SPACE eurjchem-112 73 1 furthermore furthermore ADV eurjchem-112 73 2 , , PUNCT eurjchem-112 73 3     SPACE eurjchem-112 73 4 it it PRON eurjchem-112 73 5     SPACE eurjchem-112 73 6 was be AUX eurjchem-112 73 7     SPACE eurjchem-112 73 8 used use VERB eurjchem-112 73 9     SPACE eurjchem-112 73 10 to to PART eurjchem-112 73 11     SPACE eurjchem-112 73 12 catalyze catalyze VERB eurjchem-112 73 13     SPACE eurjchem-112 73 14 the the DET eurjchem-112 73 15     SPACE eurjchem-112 73 16 coupling coupling NOUN eurjchem-112 73 17     SPACE eurjchem-112 73 18 of of ADP eurjchem-112 73 19     SPACE eurjchem-112 73 20 α‐ketoesters α‐ketoester NOUN eurjchem-112 73 21     SPACE eurjchem-112 73 22 with with ADP eurjchem-112 73 23     SPACE eurjchem-112 73 24 acrylonitrile acrylonitrile NOUN eurjchem-112 73 25     SPACE eurjchem-112 74 1 [ [ X eurjchem-112 74 2 13 13 NUM eurjchem-112 74 3 ] ] SYM eurjchem-112 74 4     SPACE eurjchem-112 74 5 and and CCONJ eurjchem-112 74 6     SPACE eurjchem-112 74 7 for for ADP eurjchem-112 74 8     SPACE eurjchem-112 74 9 the the DET eurjchem-112 74 10     SPACE eurjchem-112 74 11 dimerization dimerization NOUN eurjchem-112 74 12     SPACE eurjchem-112 74 13 of of ADP eurjchem-112 74 14     SPACE eurjchem-112 74 15 α α NOUN eurjchem-112 74 16 , , PUNCT eurjchem-112 74 17     SPACE eurjchem-112 74 18 β‐unsaturated β‐unsaturate VERB eurjchem-112 74 19     SPACE eurjchem-112 74 20 ketones ketone NOUN eurjchem-112 74 21     SPACE eurjchem-112 74 22 and and CCONJ eurjchem-112 74 23     SPACE eurjchem-112 74 24 nitriles nitrile NOUN eurjchem-112 74 25     SPACE eurjchem-112 75 1 [ [ X eurjchem-112 75 2 14 14 NUM eurjchem-112 75 3 ] ] PUNCT eurjchem-112 75 4 . . PUNCT eurjchem-112 75 5     SPACE eurjchem-112 76 1 in in ADP eurjchem-112 76 2     SPACE eurjchem-112 76 3 connection connection NOUN eurjchem-112 76 4     SPACE eurjchem-112 76 5 with with ADP eurjchem-112 76 6     SPACE eurjchem-112 76 7 our our PRON eurjchem-112 76 8     SPACE eurjchem-112 76 9 recent recent ADJ eurjchem-112 76 10     SPACE eurjchem-112 76 11 interest interest NOUN eurjchem-112 76 12     SPACE eurjchem-112 76 13 aimed aim VERB eurjchem-112 76 14     SPACE eurjchem-112 76 15 at at ADP eurjchem-112 76 16     SPACE eurjchem-112 76 17 the the DET eurjchem-112 76 18     SPACE eurjchem-112 76 19 development development NOUN eurjchem-112 76 20     SPACE eurjchem-112 76 21 of of ADP eurjchem-112 76 22     SPACE eurjchem-112 76 23 efficient efficient ADJ eurjchem-112 76 24     SPACE eurjchem-112 76 25 protocols protocol NOUN eurjchem-112 76 26     SPACE eurjchem-112 76 27 for for ADP eurjchem-112 76 28     SPACE eurjchem-112 76 29 the the DET eurjchem-112 76 30     SPACE eurjchem-112 76 31 preparation preparation NOUN eurjchem-112 76 32     SPACE eurjchem-112 76 33 of of ADP eurjchem-112 76 34     SPACE eurjchem-112 76 35 biological biological ADJ eurjchem-112 76 36     SPACE eurjchem-112 76 37 active active ADJ eurjchem-112 76 38     SPACE eurjchem-112 76 39 heterocycles heterocycle NOUN eurjchem-112 76 40     SPACE eurjchem-112 76 41 [ [ X eurjchem-112 76 42 15‐18 15‐18 NUM eurjchem-112 76 43 ] ] PUNCT eurjchem-112 76 44 , , PUNCT eurjchem-112 76 45     SPACE eurjchem-112 76 46 herein herein NOUN eurjchem-112 76 47 , , PUNCT eurjchem-112 76 48     SPACE eurjchem-112 76 49 we we PRON eurjchem-112 76 50     SPACE eurjchem-112 76 51 selected select VERB eurjchem-112 76 52     SPACE eurjchem-112 76 53 dabco dabco NOUN eurjchem-112 76 54     SPACE eurjchem-112 76 55 as as ADP eurjchem-112 76 56     SPACE eurjchem-112 76 57 a a DET eurjchem-112 76 58     SPACE eurjchem-112 76 59 catalyst catalyst NOUN eurjchem-112 76 60     SPACE eurjchem-112 76 61 to to PART eurjchem-112 76 62     SPACE eurjchem-112 76 63 synthesis synthesis NOUN eurjchem-112 76 64     SPACE eurjchem-112 76 65 of of ADP eurjchem-112 76 66     SPACE eurjchem-112 76 67 3‐cyano‐pyridines 3‐cyano‐pyridine NOUN eurjchem-112 76 68 . . PUNCT eurjchem-112 76 69     SPACE eurjchem-112 77 1 the the DET eurjchem-112 77 2     SPACE eurjchem-112 77 3 reaction reaction NOUN eurjchem-112 77 4     SPACE eurjchem-112 77 5 of of ADP eurjchem-112 77 6     SPACE eurjchem-112 77 7 various various ADJ eurjchem-112 77 8     SPACE eurjchem-112 77 9 aldehydes aldehyde NOUN eurjchem-112 77 10 , , PUNCT eurjchem-112 77 11     SPACE eurjchem-112 77 12 3,4‐dimethoxyacetophenone 3,4‐dimethoxyacetophenone NUM eurjchem-112 77 13 , , PUNCT eurjchem-112 77 14     SPACE eurjchem-112 77 15 ammonium ammonium NOUN eurjchem-112 77 16     SPACE eurjchem-112 77 17 acetate acetate NOUN eurjchem-112 77 18     SPACE eurjchem-112 77 19 and and CCONJ eurjchem-112 77 20     SPACE eurjchem-112 77 21 ethyl ethyl PROPN eurjchem-112 77 22     SPACE eurjchem-112 77 23 cyanoacetate cyanoacetate NOUN eurjchem-112 77 24     SPACE eurjchem-112 77 25 or or CCONJ eurjchem-112 77 26     SPACE eurjchem-112 77 27 malononitrile malononitrile NOUN eurjchem-112 77 28     SPACE eurjchem-112 77 29 in in ADP eurjchem-112 77 30     SPACE eurjchem-112 77 31 the the DET eurjchem-112 77 32     SPACE eurjchem-112 77 33 presence presence NOUN eurjchem-112 77 34     SPACE eurjchem-112 77 35 of of ADP eurjchem-112 77 36     SPACE eurjchem-112 77 37 dabco dabco NOUN eurjchem-112 77 38     SPACE eurjchem-112 77 39 in in ADP eurjchem-112 77 40     SPACE eurjchem-112 77 41 ethanol ethanol NOUN eurjchem-112 77 42     SPACE eurjchem-112 77 43 afforded afford VERB eurjchem-112 77 44     SPACE eurjchem-112 77 45 4‐alkyl(aryl)‐3‐ 4‐alkyl(aryl)‐3‐ NOUN eurjchem-112 77 46 cyano‐2(1h)‐iminopyridines cyano‐2(1h)‐iminopyridine NOUN eurjchem-112 77 47     SPACE eurjchem-112 77 48 and and CCONJ eurjchem-112 77 49     SPACE eurjchem-112 77 50 2(1h)‐pyridinones 2(1h)‐pyridinone NOUN eurjchem-112 77 51     SPACE eurjchem-112 77 52 in in ADP eurjchem-112 77 53     SPACE eurjchem-112 77 54 good good ADJ eurjchem-112 77 55     SPACE eurjchem-112 77 56 yields yield NOUN eurjchem-112 77 57     SPACE eurjchem-112 77 58 ( ( PUNCT eurjchem-112 77 59 table table NOUN eurjchem-112 77 60     SPACE eurjchem-112 77 61 1 1 NUM eurjchem-112 77 62 ) ) PUNCT eurjchem-112 77 63 . . PUNCT eurjchem-112 77 64     SPACE eurjchem-112 78 1 the the DET eurjchem-112 78 2     SPACE eurjchem-112 78 3 reaction reaction NOUN eurjchem-112 78 4     SPACE eurjchem-112 78 5 times time NOUN eurjchem-112 78 6     SPACE eurjchem-112 78 7 are be AUX eurjchem-112 78 8     SPACE eurjchem-112 78 9 considerably considerably ADV eurjchem-112 78 10     SPACE eurjchem-112 78 11 reduced reduce VERB eurjchem-112 78 12     SPACE eurjchem-112 78 13 with with ADP eurjchem-112 78 14     SPACE eurjchem-112 78 15 improved improve VERB eurjchem-112 78 16     SPACE eurjchem-112 78 17 yields yield NOUN eurjchem-112 78 18     SPACE eurjchem-112 78 19 as as ADP eurjchem-112 78 20     SPACE eurjchem-112 78 21 compared compare VERB eurjchem-112 78 22     SPACE eurjchem-112 78 23 to to ADP eurjchem-112 78 24     SPACE eurjchem-112 78 25 other other ADJ eurjchem-112 78 26     SPACE eurjchem-112 78 27 procedures procedure NOUN eurjchem-112 78 28 . . PUNCT eurjchem-112 78 29     SPACE eurjchem-112 79 1 the the DET eurjchem-112 79 2     SPACE eurjchem-112 79 3 amount amount NOUN eurjchem-112 79 4     SPACE eurjchem-112 79 5 of of ADP eurjchem-112 79 6     SPACE eurjchem-112 79 7 ammonium ammonium NOUN eurjchem-112 79 8     SPACE eurjchem-112 79 9 acetate acetate NOUN eurjchem-112 79 10     SPACE eurjchem-112 79 11 was be AUX eurjchem-112 79 12     SPACE eurjchem-112 79 13 adjusted adjust VERB eurjchem-112 79 14     SPACE eurjchem-112 79 15 to to PART eurjchem-112 79 16     SPACE eurjchem-112 79 17 get get VERB eurjchem-112 79 18     SPACE eurjchem-112 79 19 the the DET eurjchem-112 79 20     SPACE eurjchem-112 79 21 maximum maximum ADJ eurjchem-112 79 22     SPACE eurjchem-112 79 23 yield yield NOUN eurjchem-112 79 24     SPACE eurjchem-112 79 25 of of ADP eurjchem-112 79 26     SPACE eurjchem-112 79 27 the the DET eurjchem-112 79 28     SPACE eurjchem-112 79 29 products product NOUN eurjchem-112 79 30 . . PUNCT eurjchem-112 79 31     SPACE eurjchem-112 79 32 by by ADP eurjchem-112 79 33     SPACE eurjchem-112 79 34 carrying carry VERB eurjchem-112 79 35     SPACE eurjchem-112 79 36 out out ADP eurjchem-112 79 37     SPACE eurjchem-112 79 38 reactions reaction NOUN eurjchem-112 79 39     SPACE eurjchem-112 79 40 with with ADP eurjchem-112 79 41     SPACE eurjchem-112 79 42 different different ADJ eurjchem-112 79 43     SPACE eurjchem-112 79 44 amounts amount NOUN eurjchem-112 79 45     SPACE eurjchem-112 79 46 of of ADP eurjchem-112 79 47     SPACE eurjchem-112 79 48 ammonium ammonium NOUN eurjchem-112 79 49     SPACE eurjchem-112 79 50 acetate acetate NOUN eurjchem-112 79 51 , , PUNCT eurjchem-112 79 52     SPACE eurjchem-112 79 53 it it PRON eurjchem-112 79 54     SPACE eurjchem-112 79 55 has have AUX eurjchem-112 79 56     SPACE eurjchem-112 79 57 been be AUX eurjchem-112 79 58     SPACE eurjchem-112 79 59 found find VERB eurjchem-112 79 60     SPACE eurjchem-112 79 61 that that SCONJ eurjchem-112 79 62     SPACE eurjchem-112 79 63 8 8 NUM eurjchem-112 79 64     SPACE eurjchem-112 79 65 mmol mmol NOUN eurjchem-112 79 66     SPACE eurjchem-112 79 67 of of ADP eurjchem-112 79 68     SPACE eurjchem-112 79 69 the the DET eurjchem-112 79 70     SPACE eurjchem-112 79 71 ammonium ammonium NOUN eurjchem-112 79 72     SPACE eurjchem-112 79 73 acetate acetate NOUN eurjchem-112 79 74     SPACE eurjchem-112 79 75 furnished furnish VERB eurjchem-112 79 76     SPACE eurjchem-112 79 77 the the DET eurjchem-112 79 78     SPACE eurjchem-112 79 79 maximum maximum ADJ eurjchem-112 79 80     SPACE eurjchem-112 79 81 yield yield NOUN eurjchem-112 79 82     SPACE eurjchem-112 79 83 for for ADP eurjchem-112 79 84     SPACE eurjchem-112 79 85 1 1 NUM eurjchem-112 79 86     SPACE eurjchem-112 79 87 mmol mmol NOUN eurjchem-112 79 88     SPACE eurjchem-112 79 89 of of ADP eurjchem-112 79 90     SPACE eurjchem-112 79 91 the the DET eurjchem-112 79 92     SPACE eurjchem-112 79 93 reactants reactant NOUN eurjchem-112 79 94 . . PUNCT eurjchem-112 79 95     SPACE eurjchem-112 79 96 when when SCONJ eurjchem-112 79 97     SPACE eurjchem-112 79 98 ethyl ethyl PROPN eurjchem-112 79 99     SPACE eurjchem-112 79 100 cyanoacetate cyanoacetate NOUN eurjchem-112 79 101     SPACE eurjchem-112 79 102 was be AUX eurjchem-112 79 103     SPACE eurjchem-112 79 104 involved involve VERB eurjchem-112 79 105     SPACE eurjchem-112 79 106 instead instead ADV eurjchem-112 79 107     SPACE eurjchem-112 79 108 of of ADP eurjchem-112 79 109     SPACE eurjchem-112 79 110 malononitrile malononitrile NOUN eurjchem-112 79 111 , , PUNCT eurjchem-112 79 112     SPACE eurjchem-112 79 113 the the DET eurjchem-112 79 114     SPACE eurjchem-112 79 115 corresponding corresponding ADJ eurjchem-112 79 116     SPACE eurjchem-112 79 117 2‐1h‐ 2‐1h‐ PROPN eurjchem-112 79 118 pyridone pyridone NOUN eurjchem-112 79 119     SPACE eurjchem-112 79 120 was be AUX eurjchem-112 79 121     SPACE eurjchem-112 79 122 obtained obtain VERB eurjchem-112 79 123     SPACE eurjchem-112 79 124 in in ADP eurjchem-112 79 125     SPACE eurjchem-112 79 126 good good ADJ eurjchem-112 79 127     SPACE eurjchem-112 79 128 yield yield NOUN eurjchem-112 79 129     SPACE eurjchem-112 79 130 ( ( PUNCT eurjchem-112 79 131 table table NOUN eurjchem-112 79 132     SPACE eurjchem-112 79 133 1 1 NUM eurjchem-112 79 134 , , PUNCT eurjchem-112 79 135     SPACE eurjchem-112 79 136 entries entry NOUN eurjchem-112 79 137     SPACE eurjchem-112 79 138 6‐10 6‐10 NUM eurjchem-112 79 139 ) ) PUNCT eurjchem-112 79 140 . . PUNCT eurjchem-112 79 141     SPACE eurjchem-112 80 1 the the DET eurjchem-112 80 2     SPACE eurjchem-112 80 3 title title NOUN eurjchem-112 80 4     SPACE eurjchem-112 80 5 compounds compound NOUN eurjchem-112 80 6     SPACE eurjchem-112 80 7 were be AUX eurjchem-112 80 8     SPACE eurjchem-112 80 9 characterized characterize VERB eurjchem-112 80 10     SPACE eurjchem-112 80 11 on on ADP eurjchem-112 80 12     SPACE eurjchem-112 80 13 the the DET eurjchem-112 80 14     SPACE eurjchem-112 80 15 basis basis NOUN eurjchem-112 80 16     SPACE eurjchem-112 80 17 of of ADP eurjchem-112 80 18     SPACE eurjchem-112 80 19 analytical analytical ADJ eurjchem-112 80 20 , , PUNCT eurjchem-112 80 21       SPACE eurjchem-112 80 22 spectral spectral ADJ eurjchem-112 80 23       SPACE eurjchem-112 80 24 data data PROPN eurjchem-112 80 25       SPACE eurjchem-112 80 26 and and CCONJ eurjchem-112 80 27       SPACE eurjchem-112 80 28 by by ADP eurjchem-112 80 29       SPACE eurjchem-112 80 30 comparison comparison NOUN eurjchem-112 80 31       SPACE eurjchem-112 80 32 with with ADP eurjchem-112 80 33       SPACE eurjchem-112 80 34 authentic authentic ADJ eurjchem-112 80 35 234 234 NUM eurjchem-112 80 36     SPACE eurjchem-112 80 37 beheshtia beheshtia PROPN eurjchem-112 80 38     SPACE eurjchem-112 80 39 et et PROPN eurjchem-112 80 40     SPACE eurjchem-112 80 41 al al PROPN eurjchem-112 80 42 . . PROPN eurjchem-112 80 43     SPACE eurjchem-112 80 44 / / SYM eurjchem-112 80 45     SPACE eurjchem-112 80 46 european european ADJ eurjchem-112 80 47     SPACE eurjchem-112 80 48 journal journal NOUN eurjchem-112 80 49     SPACE eurjchem-112 80 50 of of ADP eurjchem-112 80 51     SPACE eurjchem-112 80 52 chemistry chemistry NOUN eurjchem-112 80 53     SPACE eurjchem-112 80 54 1 1 NUM eurjchem-112 80 55     SPACE eurjchem-112 80 56 ( ( PUNCT eurjchem-112 80 57 3 3 NUM eurjchem-112 80 58 ) ) PUNCT eurjchem-112 80 59     SPACE eurjchem-112 80 60 ( ( PUNCT eurjchem-112 80 61 2010 2010 NUM eurjchem-112 80 62 ) ) PUNCT eurjchem-112 80 63     SPACE eurjchem-112 80 64 232­235 232­235 NUM eurjchem-112 80 65         SPACE eurjchem-112 80 66 scheme scheme NOUN eurjchem-112 80 67     SPACE eurjchem-112 80 68 2 2 NUM eurjchem-112 80 69         SPACE eurjchem-112 80 70 samples sample NOUN eurjchem-112 80 71 . . PUNCT eurjchem-112 80 72     SPACE eurjchem-112 80 73 for for ADP eurjchem-112 80 74     SPACE eurjchem-112 80 75 the the DET eurjchem-112 80 76     SPACE eurjchem-112 80 77 aldehyde aldehyde NOUN eurjchem-112 80 78     SPACE eurjchem-112 80 79 component component NOUN eurjchem-112 80 80 , , PUNCT eurjchem-112 80 81     SPACE eurjchem-112 80 82 not not PART eurjchem-112 80 83     SPACE eurjchem-112 80 84 only only ADV eurjchem-112 80 85     SPACE eurjchem-112 80 86 aromatic aromatic NOUN eurjchem-112 80 87     SPACE eurjchem-112 80 88 but but CCONJ eurjchem-112 80 89     SPACE eurjchem-112 80 90 also also ADV eurjchem-112 80 91     SPACE eurjchem-112 80 92 aliphatic aliphatic ADJ eurjchem-112 80 93     SPACE eurjchem-112 80 94 aldehydes aldehyde NOUN eurjchem-112 80 95     SPACE eurjchem-112 80 96 proceeded proceed VERB eurjchem-112 80 97     SPACE eurjchem-112 80 98 well well ADV eurjchem-112 80 99     SPACE eurjchem-112 80 100 ( ( PUNCT eurjchem-112 80 101 table table NOUN eurjchem-112 80 102     SPACE eurjchem-112 80 103 1 1 NUM eurjchem-112 80 104 , , PUNCT eurjchem-112 80 105     SPACE eurjchem-112 80 106 entries entry NOUN eurjchem-112 80 107     SPACE eurjchem-112 80 108 1 1 NUM eurjchem-112 80 109 , , PUNCT eurjchem-112 80 110     SPACE eurjchem-112 80 111 6 6 NUM eurjchem-112 80 112 ) ) PUNCT eurjchem-112 80 113 . . PUNCT eurjchem-112 80 114     SPACE eurjchem-112 81 1 the the DET eurjchem-112 81 2     SPACE eurjchem-112 81 3 reaction reaction NOUN eurjchem-112 81 4     SPACE eurjchem-112 81 5 was be AUX eurjchem-112 81 6     SPACE eurjchem-112 81 7 conducted conduct VERB eurjchem-112 81 8     SPACE eurjchem-112 81 9 with with ADP eurjchem-112 81 10     SPACE eurjchem-112 81 11 various various ADJ eurjchem-112 81 12     SPACE eurjchem-112 81 13 solvents solvent NOUN eurjchem-112 81 14     SPACE eurjchem-112 81 15 for for ADP eurjchem-112 81 16     SPACE eurjchem-112 81 17 the the DET eurjchem-112 81 18     SPACE eurjchem-112 81 19 synthesis synthesis NOUN eurjchem-112 81 20     SPACE eurjchem-112 81 21 of of ADP eurjchem-112 81 22     SPACE eurjchem-112 81 23 5b 5b NOUN eurjchem-112 81 24     SPACE eurjchem-112 81 25 using use VERB eurjchem-112 81 26     SPACE eurjchem-112 81 27 dabco dabco NOUN eurjchem-112 81 28     SPACE eurjchem-112 81 29 as as ADP eurjchem-112 81 30     SPACE eurjchem-112 81 31 a a DET eurjchem-112 81 32     SPACE eurjchem-112 81 33 catalyst catalyst NOUN eurjchem-112 81 34 . . PUNCT eurjchem-112 81 35     SPACE eurjchem-112 82 1 as as SCONJ eurjchem-112 82 2     SPACE eurjchem-112 82 3 shown show VERB eurjchem-112 82 4     SPACE eurjchem-112 82 5 in in ADP eurjchem-112 82 6     SPACE eurjchem-112 82 7 table table NOUN eurjchem-112 82 8     SPACE eurjchem-112 82 9 2 2 NUM eurjchem-112 82 10 , , PUNCT eurjchem-112 82 11     SPACE eurjchem-112 82 12 the the DET eurjchem-112 82 13     SPACE eurjchem-112 82 14 performance performance NOUN eurjchem-112 82 15     SPACE eurjchem-112 82 16 of of ADP eurjchem-112 82 17     SPACE eurjchem-112 82 18 various various ADJ eurjchem-112 82 19     SPACE eurjchem-112 82 20 solvents solvent NOUN eurjchem-112 82 21     SPACE eurjchem-112 82 22 are be AUX eurjchem-112 82 23     SPACE eurjchem-112 82 24 in in ADP eurjchem-112 82 25     SPACE eurjchem-112 82 26 the the DET eurjchem-112 82 27     SPACE eurjchem-112 82 28 following following NOUN eurjchem-112 82 29     SPACE eurjchem-112 82 30 the the DET eurjchem-112 82 31     SPACE eurjchem-112 82 32 order order NOUN eurjchem-112 82 33 : : PUNCT eurjchem-112 82 34     SPACE eurjchem-112 82 35 ethanol ethanol NOUN eurjchem-112 82 36     SPACE eurjchem-112 82 37 > > SYM eurjchem-112 82 38     SPACE eurjchem-112 82 39 acetonitrile acetonitrile NOUN eurjchem-112 82 40     SPACE eurjchem-112 82 41 > > SYM eurjchem-112 82 42     SPACE eurjchem-112 82 43 ethyl ethyl PROPN eurjchem-112 82 44     SPACE eurjchem-112 82 45 acetate acetate NOUN eurjchem-112 82 46     SPACE eurjchem-112 82 47 > > SYM eurjchem-112 82 48     SPACE eurjchem-112 82 49 thf thf NOUN eurjchem-112 82 50     SPACE eurjchem-112 82 51 > > NOUN eurjchem-112 82 52     SPACE eurjchem-112 82 53 dichloromethane dichloromethane NOUN eurjchem-112 82 54 . . PUNCT eurjchem-112 82 55     SPACE eurjchem-112 82 56 ethanol ethanol NOUN eurjchem-112 82 57     SPACE eurjchem-112 82 58 provided provide VERB eurjchem-112 82 59     SPACE eurjchem-112 82 60 better well ADJ eurjchem-112 82 61     SPACE eurjchem-112 82 62 yields yield NOUN eurjchem-112 82 63     SPACE eurjchem-112 82 64 compared compare VERB eurjchem-112 82 65     SPACE eurjchem-112 82 66 to to ADP eurjchem-112 82 67     SPACE eurjchem-112 82 68 other other ADJ eurjchem-112 82 69     SPACE eurjchem-112 82 70 solvents solvent NOUN eurjchem-112 82 71 . . PUNCT eurjchem-112 82 72     SPACE eurjchem-112 82 73 in in ADP eurjchem-112 82 74     SPACE eurjchem-112 82 75 addition addition NOUN eurjchem-112 82 76 , , PUNCT eurjchem-112 82 77     SPACE eurjchem-112 82 78 the the DET eurjchem-112 82 79     SPACE eurjchem-112 82 80 time time NOUN eurjchem-112 82 81     SPACE eurjchem-112 82 82 required require VERB eurjchem-112 82 83     SPACE eurjchem-112 82 84 for for ADP eurjchem-112 82 85     SPACE eurjchem-112 82 86 completion completion NOUN eurjchem-112 82 87     SPACE eurjchem-112 82 88 of of ADP eurjchem-112 82 89     SPACE eurjchem-112 82 90 the the DET eurjchem-112 82 91     SPACE eurjchem-112 82 92 reaction reaction NOUN eurjchem-112 82 93     SPACE eurjchem-112 82 94 was be AUX eurjchem-112 82 95     SPACE eurjchem-112 82 96 found find VERB eurjchem-112 82 97     SPACE eurjchem-112 82 98 to to PART eurjchem-112 82 99     SPACE eurjchem-112 82 100 be be AUX eurjchem-112 82 101     SPACE eurjchem-112 82 102 less less ADJ eurjchem-112 82 103     SPACE eurjchem-112 82 104 in in ADP eurjchem-112 82 105     SPACE eurjchem-112 82 106 ethanol ethanol NOUN eurjchem-112 82 107 . . PUNCT eurjchem-112 82 108           SPACE eurjchem-112 83 1 table table NOUN eurjchem-112 83 2     SPACE eurjchem-112 83 3 2 2 NUM eurjchem-112 83 4 . . PUNCT eurjchem-112 83 5     SPACE eurjchem-112 83 6 synthesis synthesis NOUN eurjchem-112 83 7     SPACE eurjchem-112 83 8 of of ADP eurjchem-112 83 9     SPACE eurjchem-112 83 10 5b 5b NOUN eurjchem-112 83 11     SPACE eurjchem-112 83 12 with with ADP eurjchem-112 83 13     SPACE eurjchem-112 83 14 dabco dabco NOUN eurjchem-112 83 15     SPACE eurjchem-112 83 16 in in ADP eurjchem-112 83 17     SPACE eurjchem-112 83 18 the the DET eurjchem-112 83 19     SPACE eurjchem-112 83 20 presence presence NOUN eurjchem-112 83 21     SPACE eurjchem-112 83 22 of of ADP eurjchem-112 83 23     SPACE eurjchem-112 83 24 different different ADJ eurjchem-112 83 25     SPACE eurjchem-112 83 26 solvents solvent NOUN eurjchem-112 83 27 . . PUNCT eurjchem-112 83 28     SPACE eurjchem-112 83 29 entry entry NOUN eurjchem-112 83 30     SPACE eurjchem-112 83 31 solvent solvent NOUN eurjchem-112 83 32     SPACE eurjchem-112 83 33 temperature temperature NOUN eurjchem-112 83 34     SPACE eurjchem-112 83 35 time(h time(h NOUN eurjchem-112 83 36 ) ) PUNCT eurjchem-112 83 37     SPACE eurjchem-112 83 38 yield(%)a yield(%)a PROPN eurjchem-112 83 39     SPACE eurjchem-112 83 40 1 1 NUM eurjchem-112 83 41     SPACE eurjchem-112 83 42 ethanol ethanol NOUN eurjchem-112 83 43     SPACE eurjchem-112 83 44 reflux reflux NOUN eurjchem-112 83 45     SPACE eurjchem-112 83 46 3 3 NUM eurjchem-112 83 47     SPACE eurjchem-112 83 48 91 91 NUM eurjchem-112 83 49 2 2 NUM eurjchem-112 83 50     SPACE eurjchem-112 83 51 acetonitrile acetonitrile NOUN eurjchem-112 83 52     SPACE eurjchem-112 83 53 reflux reflux NOUN eurjchem-112 83 54     SPACE eurjchem-112 83 55 3 3 NUM eurjchem-112 83 56     SPACE eurjchem-112 83 57 84 84 NUM eurjchem-112 83 58 3 3 NUM eurjchem-112 83 59     SPACE eurjchem-112 83 60 ethyl ethyl PROPN eurjchem-112 83 61     SPACE eurjchem-112 83 62 acetate acetate NOUN eurjchem-112 83 63     SPACE eurjchem-112 83 64 reflux reflux NOUN eurjchem-112 83 65     SPACE eurjchem-112 83 66 4 4 NUM eurjchem-112 83 67     SPACE eurjchem-112 83 68 82 82 NUM eurjchem-112 83 69 4 4 NUM eurjchem-112 83 70     SPACE eurjchem-112 83 71 thf thf NOUN eurjchem-112 83 72     SPACE eurjchem-112 83 73 reflux reflux NOUN eurjchem-112 83 74     SPACE eurjchem-112 83 75 4 4 NUM eurjchem-112 83 76     SPACE eurjchem-112 83 77 78 78 NUM eurjchem-112 83 78 5 5 NUM eurjchem-112 83 79     SPACE eurjchem-112 83 80 dichloromethane dichloromethane NOUN eurjchem-112 83 81     SPACE eurjchem-112 83 82 reflux reflux NOUN eurjchem-112 83 83     SPACE eurjchem-112 83 84 6 6 NUM eurjchem-112 83 85     SPACE eurjchem-112 83 86 65 65 NUM eurjchem-112 83 87 ayield ayield NOUN eurjchem-112 83 88     SPACE eurjchem-112 83 89 of of ADP eurjchem-112 83 90     SPACE eurjchem-112 83 91 isolated isolated ADJ eurjchem-112 83 92     SPACE eurjchem-112 83 93 products product NOUN eurjchem-112 83 94 . . PUNCT eurjchem-112 83 95         SPACE eurjchem-112 84 1 the the DET eurjchem-112 84 2     SPACE eurjchem-112 84 3 effect effect NOUN eurjchem-112 84 4     SPACE eurjchem-112 84 5 of of ADP eurjchem-112 84 6     SPACE eurjchem-112 84 7 temperature temperature NOUN eurjchem-112 84 8     SPACE eurjchem-112 84 9 in in ADP eurjchem-112 84 10     SPACE eurjchem-112 84 11 ethanol ethanol NOUN eurjchem-112 84 12     SPACE eurjchem-112 84 13 as as SCONJ eurjchem-112 84 14     SPACE eurjchem-112 84 15 a a DET eurjchem-112 84 16     SPACE eurjchem-112 84 17 solvent solvent NOUN eurjchem-112 84 18     SPACE eurjchem-112 84 19 was be AUX eurjchem-112 84 20     SPACE eurjchem-112 84 21 studied study VERB eurjchem-112 84 22     SPACE eurjchem-112 84 23 by by ADP eurjchem-112 84 24     SPACE eurjchem-112 84 25 carrying carry VERB eurjchem-112 84 26     SPACE eurjchem-112 84 27 out out ADP eurjchem-112 84 28     SPACE eurjchem-112 84 29 the the DET eurjchem-112 84 30     SPACE eurjchem-112 84 31 reactions reaction NOUN eurjchem-112 84 32     SPACE eurjchem-112 84 33 at at ADP eurjchem-112 84 34     SPACE eurjchem-112 84 35 different different ADJ eurjchem-112 84 36     SPACE eurjchem-112 84 37 temperatures temperature NOUN eurjchem-112 84 38     SPACE eurjchem-112 84 39 [ [ X eurjchem-112 84 40 room room NOUN eurjchem-112 84 41     SPACE eurjchem-112 84 42 temperature temperature NOUN eurjchem-112 84 43     SPACE eurjchem-112 84 44 ( ( PUNCT eurjchem-112 84 45 25 25 NUM eurjchem-112 84 46     SPACE eurjchem-112 84 47 oc oc NOUN eurjchem-112 84 48 ) ) PUNCT eurjchem-112 84 49 , , PUNCT eurjchem-112 84 50     SPACE eurjchem-112 84 51 45 45 NUM eurjchem-112 84 52     SPACE eurjchem-112 84 53 oc oc NOUN eurjchem-112 84 54     SPACE eurjchem-112 84 55 and and CCONJ eurjchem-112 84 56     SPACE eurjchem-112 84 57 under under ADP eurjchem-112 84 58     SPACE eurjchem-112 84 59 refluxing refluxing NOUN eurjchem-112 84 60     SPACE eurjchem-112 84 61 temperature temperature NOUN eurjchem-112 84 62     SPACE eurjchem-112 84 63 ( ( PUNCT eurjchem-112 84 64 78 78 NUM eurjchem-112 84 65     SPACE eurjchem-112 84 66 oc oc NOUN eurjchem-112 84 67 ) ) PUNCT eurjchem-112 84 68 ] ] PUNCT eurjchem-112 84 69 . . PUNCT eurjchem-112 84 70     SPACE eurjchem-112 84 71 as as SCONJ eurjchem-112 84 72     SPACE eurjchem-112 84 73 shown show VERB eurjchem-112 84 74     SPACE eurjchem-112 84 75 in in ADP eurjchem-112 84 76     SPACE eurjchem-112 84 77 table table NOUN eurjchem-112 84 78     SPACE eurjchem-112 84 79 1 1 NUM eurjchem-112 84 80 , , PUNCT eurjchem-112 84 81     SPACE eurjchem-112 84 82 the the DET eurjchem-112 84 83     SPACE eurjchem-112 84 84 yields yield NOUN eurjchem-112 84 85     SPACE eurjchem-112 84 86 of of ADP eurjchem-112 84 87     SPACE eurjchem-112 84 88 reactions reaction NOUN eurjchem-112 84 89     SPACE eurjchem-112 84 90 increased increase VERB eurjchem-112 84 91     SPACE eurjchem-112 84 92 as as SCONJ eurjchem-112 84 93     SPACE eurjchem-112 84 94 the the DET eurjchem-112 84 95     SPACE eurjchem-112 84 96 reaction reaction NOUN eurjchem-112 84 97     SPACE eurjchem-112 84 98 temperature temperature NOUN eurjchem-112 84 99     SPACE eurjchem-112 84 100 was be AUX eurjchem-112 84 101     SPACE eurjchem-112 84 102 raised raise VERB eurjchem-112 84 103 . . PUNCT eurjchem-112 84 104     SPACE eurjchem-112 84 105 from from ADP eurjchem-112 84 106     SPACE eurjchem-112 84 107 these these DET eurjchem-112 84 108     SPACE eurjchem-112 84 109 results result NOUN eurjchem-112 84 110 , , PUNCT eurjchem-112 84 111     SPACE eurjchem-112 84 112 it it PRON eurjchem-112 84 113     SPACE eurjchem-112 84 114 was be AUX eurjchem-112 84 115     SPACE eurjchem-112 84 116 decided decide VERB eurjchem-112 84 117     SPACE eurjchem-112 84 118 that that SCONJ eurjchem-112 84 119     SPACE eurjchem-112 84 120 refluxing refluxing NOUN eurjchem-112 84 121     SPACE eurjchem-112 84 122 temperature temperature NOUN eurjchem-112 84 123     SPACE eurjchem-112 84 124 would would AUX eurjchem-112 84 125     SPACE eurjchem-112 84 126 be be AUX eurjchem-112 84 127     SPACE eurjchem-112 84 128 the the DET eurjchem-112 84 129     SPACE eurjchem-112 84 130 best good ADJ eurjchem-112 84 131     SPACE eurjchem-112 84 132 temperature temperature NOUN eurjchem-112 84 133     SPACE eurjchem-112 84 134 for for ADP eurjchem-112 84 135     SPACE eurjchem-112 84 136 all all DET eurjchem-112 84 137     SPACE eurjchem-112 84 138 reactions reaction NOUN eurjchem-112 84 139 . . PUNCT eurjchem-112 84 140     SPACE eurjchem-112 85 1 the the DET eurjchem-112 85 2     SPACE eurjchem-112 85 3 reaction reaction NOUN eurjchem-112 85 4     SPACE eurjchem-112 85 5 proceeds proceed VERB eurjchem-112 85 6     SPACE eurjchem-112 85 7 very very ADV eurjchem-112 85 8     SPACE eurjchem-112 85 9 cleanly cleanly ADV eurjchem-112 85 10     SPACE eurjchem-112 85 11 under under ADV eurjchem-112 85 12     SPACE eurjchem-112 85 13 reflux reflux NOUN eurjchem-112 85 14     SPACE eurjchem-112 85 15 condition condition NOUN eurjchem-112 85 16     SPACE eurjchem-112 85 17 and and CCONJ eurjchem-112 85 18     SPACE eurjchem-112 85 19 free free ADJ eurjchem-112 85 20     SPACE eurjchem-112 85 21 of of ADP eurjchem-112 85 22     SPACE eurjchem-112 85 23 side side NOUN eurjchem-112 85 24     SPACE eurjchem-112 85 25 products product NOUN eurjchem-112 85 26 . . PUNCT eurjchem-112 85 27     SPACE eurjchem-112 86 1 the the DET eurjchem-112 86 2     SPACE eurjchem-112 86 3 reasonable reasonable ADJ eurjchem-112 86 4     SPACE eurjchem-112 86 5 mechanism mechanism NOUN eurjchem-112 86 6     SPACE eurjchem-112 86 7 for for ADP eurjchem-112 86 8     SPACE eurjchem-112 86 9 this this DET eurjchem-112 86 10     SPACE eurjchem-112 86 11 reaction reaction NOUN eurjchem-112 86 12     SPACE eurjchem-112 86 13 has have AUX eurjchem-112 86 14     SPACE eurjchem-112 86 15 been be AUX eurjchem-112 86 16     SPACE eurjchem-112 86 17 suggested suggest VERB eurjchem-112 86 18     SPACE eurjchem-112 86 19 in in ADP eurjchem-112 86 20     SPACE eurjchem-112 86 21 scheme scheme NOUN eurjchem-112 86 22     SPACE eurjchem-112 86 23 2 2 NUM eurjchem-112 86 24 . . PUNCT eurjchem-112 86 25     SPACE eurjchem-112 86 26 the the DET eurjchem-112 86 27     SPACE eurjchem-112 86 28 first first ADJ eurjchem-112 86 29     SPACE eurjchem-112 86 30 step step NOUN eurjchem-112 86 31     SPACE eurjchem-112 86 32 may may AUX eurjchem-112 86 33     SPACE eurjchem-112 86 34 involve involve VERB eurjchem-112 86 35     SPACE eurjchem-112 86 36 condensation condensation NOUN eurjchem-112 86 37     SPACE eurjchem-112 86 38 reaction reaction NOUN eurjchem-112 86 39     SPACE eurjchem-112 86 40 of of ADP eurjchem-112 86 41     SPACE eurjchem-112 86 42 malononitrile malononitrile NOUN eurjchem-112 86 43     SPACE eurjchem-112 86 44 or or CCONJ eurjchem-112 86 45     SPACE eurjchem-112 86 46 ethyl ethyl NOUN eurjchem-112 86 47     SPACE eurjchem-112 86 48 cyanoacetate cyanoacetate NOUN eurjchem-112 86 49     SPACE eurjchem-112 86 50 with with ADP eurjchem-112 86 51     SPACE eurjchem-112 86 52 the the DET eurjchem-112 86 53     SPACE eurjchem-112 86 54 aromatic aromatic ADJ eurjchem-112 86 55     SPACE eurjchem-112 86 56 aldehyde aldehyde NOUN eurjchem-112 86 57 , , PUNCT eurjchem-112 86 58     SPACE eurjchem-112 86 59 followed follow VERB eurjchem-112 86 60     SPACE eurjchem-112 86 61 by by ADP eurjchem-112 86 62     SPACE eurjchem-112 86 63 attack attack NOUN eurjchem-112 86 64     SPACE eurjchem-112 86 65 of of ADP eurjchem-112 86 66     SPACE eurjchem-112 86 67 9 9 NUM eurjchem-112 86 68     SPACE eurjchem-112 86 69 to to ADP eurjchem-112 86 70     SPACE eurjchem-112 86 71 this this DET eurjchem-112 86 72     SPACE eurjchem-112 86 73 intermediate intermediate ADJ eurjchem-112 86 74     SPACE eurjchem-112 86 75 which which PRON eurjchem-112 86 76     SPACE eurjchem-112 86 77 after after ADP eurjchem-112 86 78     SPACE eurjchem-112 86 79 a a DET eurjchem-112 86 80     SPACE eurjchem-112 86 81 cyclization cyclization NOUN eurjchem-112 86 82     SPACE eurjchem-112 86 83 give give NOUN eurjchem-112 86 84     SPACE eurjchem-112 86 85 intermediate intermediate ADJ eurjchem-112 86 86     SPACE eurjchem-112 86 87 12 12 NUM eurjchem-112 86 88 . . PUNCT eurjchem-112 86 89     SPACE eurjchem-112 87 1 following follow VERB eurjchem-112 87 2     SPACE eurjchem-112 87 3 oxidative oxidative ADJ eurjchem-112 87 4     SPACE eurjchem-112 87 5 dehydrogenation dehydrogenation NOUN eurjchem-112 87 6     SPACE eurjchem-112 87 7 by by ADP eurjchem-112 87 8     SPACE eurjchem-112 87 9 o2 o2 PROPN eurjchem-112 87 10     SPACE eurjchem-112 87 11 [ [ X eurjchem-112 87 12 19 19 NUM eurjchem-112 87 13 ] ] PUNCT eurjchem-112 87 14 , , PUNCT eurjchem-112 87 15     SPACE eurjchem-112 87 16 the the DET eurjchem-112 87 17     SPACE eurjchem-112 87 18 desired desire VERB eurjchem-112 87 19     SPACE eurjchem-112 87 20 heterocyclic heterocyclic ADJ eurjchem-112 87 21     SPACE eurjchem-112 87 22 product product NOUN eurjchem-112 87 23     SPACE eurjchem-112 87 24 5 5 NUM eurjchem-112 87 25     SPACE eurjchem-112 87 26 is be AUX eurjchem-112 87 27     SPACE eurjchem-112 87 28 obtained obtain VERB eurjchem-112 87 29 . . PUNCT eurjchem-112 87 30     SPACE eurjchem-112 87 31 dabco dabco PROPN eurjchem-112 87 32     SPACE eurjchem-112 87 33 probably probably ADV eurjchem-112 87 34     SPACE eurjchem-112 87 35 induces induce VERB eurjchem-112 87 36     SPACE eurjchem-112 87 37 polarization polarization NOUN eurjchem-112 87 38     SPACE eurjchem-112 87 39 of of ADP eurjchem-112 87 40     SPACE eurjchem-112 87 41 carbonyl carbonyl NOUN eurjchem-112 87 42     SPACE eurjchem-112 87 43 group group NOUN eurjchem-112 87 44     SPACE eurjchem-112 87 45 in in ADP eurjchem-112 87 46     SPACE eurjchem-112 87 47 keton keton NOUN eurjchem-112 87 48     SPACE eurjchem-112 87 49 1 1 NUM eurjchem-112 87 50 . . PUNCT eurjchem-112 87 51     SPACE eurjchem-112 87 52 then then ADV eurjchem-112 87 53     SPACE eurjchem-112 87 54 nucleophilic nucleophilic ADJ eurjchem-112 87 55     SPACE eurjchem-112 87 56 attack attack NOUN eurjchem-112 87 57     SPACE eurjchem-112 87 58 of of ADP eurjchem-112 87 59     SPACE eurjchem-112 87 60 the the DET eurjchem-112 87 61     SPACE eurjchem-112 87 62 nitrogen nitrogen NOUN eurjchem-112 87 63     SPACE eurjchem-112 87 64 of of ADP eurjchem-112 87 65     SPACE eurjchem-112 87 66 ammonia ammonia NOUN eurjchem-112 87 67     SPACE eurjchem-112 87 68 obtained obtain VERB eurjchem-112 87 69     SPACE eurjchem-112 87 70 from from ADP eurjchem-112 87 71     SPACE eurjchem-112 87 72 ammonium ammonium NOUN eurjchem-112 87 73     SPACE eurjchem-112 87 74 acetate acetate NOUN eurjchem-112 87 75 , , PUNCT eurjchem-112 87 76     SPACE eurjchem-112 87 77 on on ADP eurjchem-112 87 78     SPACE eurjchem-112 87 79 activated activated ADJ eurjchem-112 87 80     SPACE eurjchem-112 87 81 carbonyl carbonyl NOUN eurjchem-112 87 82 , , PUNCT eurjchem-112 87 83     SPACE eurjchem-112 87 84 results result VERB eurjchem-112 87 85     SPACE eurjchem-112 87 86 the the DET eurjchem-112 87 87     SPACE eurjchem-112 87 88 formation formation NOUN eurjchem-112 87 89     SPACE eurjchem-112 87 90 of of ADP eurjchem-112 87 91     SPACE eurjchem-112 87 92 imino imino NOUN eurjchem-112 87 93     SPACE eurjchem-112 87 94 keone keone NOUN eurjchem-112 87 95     SPACE eurjchem-112 87 96 8 8 NUM eurjchem-112 87 97 . . PUNCT eurjchem-112 87 98     SPACE eurjchem-112 87 99 to to PART eurjchem-112 87 100     SPACE eurjchem-112 87 101 show show VERB eurjchem-112 87 102     SPACE eurjchem-112 87 103 the the DET eurjchem-112 87 104     SPACE eurjchem-112 87 105 merits merit NOUN eurjchem-112 87 106     SPACE eurjchem-112 87 107 and and CCONJ eurjchem-112 87 108     SPACE eurjchem-112 87 109 advantages advantage NOUN eurjchem-112 87 110     SPACE eurjchem-112 87 111 of of ADP eurjchem-112 87 112     SPACE eurjchem-112 87 113 using use VERB eurjchem-112 87 114     SPACE eurjchem-112 87 115 dabco dabco NOUN eurjchem-112 87 116     SPACE eurjchem-112 87 117 as as ADP eurjchem-112 87 118     SPACE eurjchem-112 87 119 a a DET eurjchem-112 87 120     SPACE eurjchem-112 87 121 catalyst catalyst NOUN eurjchem-112 87 122 , , PUNCT eurjchem-112 87 123     SPACE eurjchem-112 87 124 our our PRON eurjchem-112 87 125     SPACE eurjchem-112 87 126 method method NOUN eurjchem-112 87 127     SPACE eurjchem-112 87 128 is be AUX eurjchem-112 87 129     SPACE eurjchem-112 87 130 compared compare VERB eurjchem-112 87 131     SPACE eurjchem-112 87 132 with with ADP eurjchem-112 87 133     SPACE eurjchem-112 87 134 reported report VERB eurjchem-112 87 135     SPACE eurjchem-112 87 136 reactions reaction NOUN eurjchem-112 87 137     SPACE eurjchem-112 87 138 ( ( PUNCT eurjchem-112 87 139 table table NOUN eurjchem-112 87 140     SPACE eurjchem-112 87 141 3 3 NUM eurjchem-112 87 142 ) ) PUNCT eurjchem-112 87 143 . . PUNCT eurjchem-112 87 144     SPACE eurjchem-112 88 1 the the DET eurjchem-112 88 2     SPACE eurjchem-112 88 3 reaction reaction NOUN eurjchem-112 88 4     SPACE eurjchem-112 88 5 results result VERB eurjchem-112 88 6     SPACE eurjchem-112 88 7 without without ADP eurjchem-112 88 8     SPACE eurjchem-112 88 9 catalyst catalyst NOUN eurjchem-112 88 10     SPACE eurjchem-112 88 11 decrease decrease NOUN eurjchem-112 88 12     SPACE eurjchem-112 88 13 and and CCONJ eurjchem-112 88 14     SPACE eurjchem-112 88 15 the the DET eurjchem-112 88 16     SPACE eurjchem-112 88 17 reaction reaction NOUN eurjchem-112 88 18     SPACE eurjchem-112 88 19 time time NOUN eurjchem-112 88 20     SPACE eurjchem-112 88 21 increases increase NOUN eurjchem-112 88 22 . . PUNCT eurjchem-112 88 23           SPACE eurjchem-112 88 24 table table NOUN eurjchem-112 88 25     SPACE eurjchem-112 88 26 3 3 NUM eurjchem-112 88 27 . . PUNCT eurjchem-112 88 28     SPACE eurjchem-112 88 29 comparision comparision NOUN eurjchem-112 88 30     SPACE eurjchem-112 88 31 of of ADP eurjchem-112 88 32     SPACE eurjchem-112 88 33 various various ADJ eurjchem-112 88 34     SPACE eurjchem-112 88 35 catalysts catalyst NOUN eurjchem-112 88 36     SPACE eurjchem-112 88 37 for for ADP eurjchem-112 88 38     SPACE eurjchem-112 88 39 the the DET eurjchem-112 88 40     SPACE eurjchem-112 88 41 synthesis synthesis NOUN eurjchem-112 88 42     SPACE eurjchem-112 88 43 of of ADP eurjchem-112 88 44                                                                 SPACE eurjchem-112 88 45 3‐cyanopyridines 3‐cyanopyridine NOUN eurjchem-112 88 46     SPACE eurjchem-112 88 47 ( ( PUNCT eurjchem-112 88 48 5b 5b NUM eurjchem-112 88 49 , , PUNCT eurjchem-112 88 50     SPACE eurjchem-112 88 51 6b 6b NOUN eurjchem-112 88 52 ) ) PUNCT eurjchem-112 88 53 . . PUNCT eurjchem-112 88 54     SPACE eurjchem-112 88 55 entry entry NOUN eurjchem-112 88 56     SPACE eurjchem-112 88 57 product product NOUN eurjchem-112 88 58     SPACE eurjchem-112 88 59 catalyst catalyst NOUN eurjchem-112 88 60     SPACE eurjchem-112 88 61 time time NOUN eurjchem-112 88 62     SPACE eurjchem-112 88 63 yield(% yield(% NOUN eurjchem-112 88 64 ) ) PUNCT eurjchem-112 88 65     SPACE eurjchem-112 88 66 ref ref NOUN eurjchem-112 88 67 . . PUNCT eurjchem-112 89 1 1 1 NUM eurjchem-112 89 2 5b 5b NUM eurjchem-112 89 3 none none NOUN eurjchem-112 89 4 6h 6h NOUN eurjchem-112 89 5     SPACE eurjchem-112 89 6 33 33 NUM eurjchem-112 89 7     SPACE eurjchem-112 89 8 20 20 NUM eurjchem-112 89 9 2 2 NUM eurjchem-112 89 10 5b 5b NUM eurjchem-112 89 11 h14[nap5w30o110 h14[nap5w30o110 PROPN eurjchem-112 89 12 ] ] X eurjchem-112 89 13     SPACE eurjchem-112 89 14 3h 3h NUM eurjchem-112 89 15     SPACE eurjchem-112 89 16 90 90 NUM eurjchem-112 89 17     SPACE eurjchem-112 89 18 21 21 NUM eurjchem-112 89 19 3 3 NUM eurjchem-112 89 20     SPACE eurjchem-112 89 21 5b 5b NUM eurjchem-112 89 22     SPACE eurjchem-112 89 23 dabco dabco NOUN eurjchem-112 89 24     SPACE eurjchem-112 89 25 2h 2h NUM eurjchem-112 89 26     SPACE eurjchem-112 89 27 91 91 NUM eurjchem-112 89 28     SPACE eurjchem-112 89 29 this this DET eurjchem-112 89 30     SPACE eurjchem-112 89 31 article article NOUN eurjchem-112 89 32 4 4 NUM eurjchem-112 89 33 6b 6b NOUN eurjchem-112 89 34 none none NOUN eurjchem-112 89 35 6h 6h NUM eurjchem-112 89 36     SPACE eurjchem-112 89 37 33 33 NUM eurjchem-112 89 38     SPACE eurjchem-112 89 39 20 20 NUM eurjchem-112 89 40 5 5 NUM eurjchem-112 89 41 6b 6b NUM eurjchem-112 89 42 h14[nap5w30o110 h14[nap5w30o110 PROPN eurjchem-112 89 43 ] ] X eurjchem-112 89 44     SPACE eurjchem-112 89 45 3h 3h NUM eurjchem-112 89 46     SPACE eurjchem-112 89 47 93 93 NUM eurjchem-112 89 48     SPACE eurjchem-112 89 49 21 21 NUM eurjchem-112 89 50 6 6 NUM eurjchem-112 89 51     SPACE eurjchem-112 89 52 6b 6b NOUN eurjchem-112 89 53     SPACE eurjchem-112 89 54 dabco dabco NOUN eurjchem-112 89 55     SPACE eurjchem-112 89 56 2h 2h NUM eurjchem-112 89 57     SPACE eurjchem-112 89 58 94 94 NUM eurjchem-112 89 59     SPACE eurjchem-112 89 60 this this DET eurjchem-112 89 61     SPACE eurjchem-112 89 62 article article NOUN eurjchem-112 89 63         SPACE eurjchem-112 89 64 beheshtia beheshtia PROPN eurjchem-112 89 65     SPACE eurjchem-112 89 66 et et PROPN eurjchem-112 89 67     SPACE eurjchem-112 89 68 al al PROPN eurjchem-112 89 69 . . PROPN eurjchem-112 89 70     SPACE eurjchem-112 89 71 / / SYM eurjchem-112 89 72     SPACE eurjchem-112 89 73 european european ADJ eurjchem-112 89 74     SPACE eurjchem-112 89 75 journal journal NOUN eurjchem-112 89 76     SPACE eurjchem-112 89 77 of of ADP eurjchem-112 89 78     SPACE eurjchem-112 89 79 chemistry chemistry NOUN eurjchem-112 89 80     SPACE eurjchem-112 89 81 1 1 NUM eurjchem-112 89 82     SPACE eurjchem-112 89 83 ( ( PUNCT eurjchem-112 89 84 3 3 NUM eurjchem-112 89 85 ) ) PUNCT eurjchem-112 89 86     SPACE eurjchem-112 89 87 ( ( PUNCT eurjchem-112 89 88 2010 2010 NUM eurjchem-112 89 89 ) ) PUNCT eurjchem-112 89 90     SPACE eurjchem-112 89 91 232­235 232­235 NUM eurjchem-112 89 92     SPACE eurjchem-112 89 93 235 235 NUM eurjchem-112 89 94         SPACE eurjchem-112 89 95 4 4 NUM eurjchem-112 89 96 . . PUNCT eurjchem-112 89 97     SPACE eurjchem-112 90 1 conclusions conclusion NOUN eurjchem-112 90 2         SPACE eurjchem-112 90 3 in in ADP eurjchem-112 90 4     SPACE eurjchem-112 90 5 summary summary NOUN eurjchem-112 90 6 , , PUNCT eurjchem-112 90 7     SPACE eurjchem-112 90 8 this this DET eurjchem-112 90 9     SPACE eurjchem-112 90 10 method method NOUN eurjchem-112 90 11     SPACE eurjchem-112 90 12 not not PART eurjchem-112 90 13     SPACE eurjchem-112 90 14 only only ADV eurjchem-112 90 15     SPACE eurjchem-112 90 16 affords afford NOUN eurjchem-112 90 17     SPACE eurjchem-112 90 18 the the DET eurjchem-112 90 19     SPACE eurjchem-112 90 20 products product NOUN eurjchem-112 90 21     SPACE eurjchem-112 90 22 in in ADP eurjchem-112 90 23     SPACE eurjchem-112 90 24 excellent excellent ADJ eurjchem-112 90 25     SPACE eurjchem-112 90 26 yields yield NOUN eurjchem-112 90 27     SPACE eurjchem-112 90 28 but but CCONJ eurjchem-112 90 29     SPACE eurjchem-112 90 30 also also ADV eurjchem-112 90 31     SPACE eurjchem-112 90 32 avoids avoid VERB eurjchem-112 90 33     SPACE eurjchem-112 90 34 the the DET eurjchem-112 90 35     SPACE eurjchem-112 90 36 problems problem NOUN eurjchem-112 90 37     SPACE eurjchem-112 90 38 associated associate VERB eurjchem-112 90 39     SPACE eurjchem-112 90 40 with with ADP eurjchem-112 90 41     SPACE eurjchem-112 90 42 catalyst catalyst NOUN eurjchem-112 90 43     SPACE eurjchem-112 90 44 cost cost NOUN eurjchem-112 90 45 , , PUNCT eurjchem-112 90 46     SPACE eurjchem-112 90 47 handling handling NOUN eurjchem-112 90 48 , , PUNCT eurjchem-112 90 49     SPACE eurjchem-112 90 50 safety safety NOUN eurjchem-112 90 51     SPACE eurjchem-112 90 52 and and CCONJ eurjchem-112 90 53     SPACE eurjchem-112 90 54 pollution pollution NOUN eurjchem-112 90 55 . . PUNCT eurjchem-112 90 56     SPACE eurjchem-112 90 57 this this DET eurjchem-112 90 58     SPACE eurjchem-112 90 59 catalyst catalyst NOUN eurjchem-112 90 60     SPACE eurjchem-112 90 61 can can AUX eurjchem-112 90 62     SPACE eurjchem-112 90 63 act act VERB eurjchem-112 90 64     SPACE eurjchem-112 90 65 as as ADP eurjchem-112 90 66     SPACE eurjchem-112 90 67 eco‐friendly eco‐friendly ADV eurjchem-112 90 68     SPACE eurjchem-112 90 69 for for ADP eurjchem-112 90 70     SPACE eurjchem-112 90 71 a a DET eurjchem-112 90 72     SPACE eurjchem-112 90 73 variety variety NOUN eurjchem-112 90 74     SPACE eurjchem-112 90 75 of of ADP eurjchem-112 90 76     SPACE eurjchem-112 90 77 organic organic ADJ eurjchem-112 90 78     SPACE eurjchem-112 90 79 transformations transformation NOUN eurjchem-112 90 80 , , PUNCT eurjchem-112 90 81     SPACE eurjchem-112 90 82 non‐volatile non‐volatile ADP eurjchem-112 90 83 , , PUNCT eurjchem-112 90 84     SPACE eurjchem-112 90 85 recyclable recyclable ADJ eurjchem-112 90 86 , , PUNCT eurjchem-112 90 87     SPACE eurjchem-112 90 88 non‐explosive non‐explosive NUM eurjchem-112 90 89 , , PUNCT eurjchem-112 90 90     SPACE eurjchem-112 90 91 easy easy ADJ eurjchem-112 90 92     SPACE eurjchem-112 90 93 to to PART eurjchem-112 90 94     SPACE eurjchem-112 90 95 handle handle VERB eurjchem-112 90 96     SPACE eurjchem-112 90 97 and and CCONJ eurjchem-112 90 98     SPACE eurjchem-112 90 99 thermally thermally ADV eurjchem-112 90 100     SPACE eurjchem-112 90 101 stable stable ADJ eurjchem-112 90 102 . . PUNCT eurjchem-112 90 103     SPACE eurjchem-112 90 104 in in ADP eurjchem-112 90 105     SPACE eurjchem-112 90 106 view view NOUN eurjchem-112 90 107     SPACE eurjchem-112 90 108 of of ADP eurjchem-112 90 109     SPACE eurjchem-112 90 110 the the DET eurjchem-112 90 111     SPACE eurjchem-112 90 112 emerging emerge VERB eurjchem-112 90 113     SPACE eurjchem-112 90 114 importance importance NOUN eurjchem-112 90 115     SPACE eurjchem-112 90 116 of of ADP eurjchem-112 90 117     SPACE eurjchem-112 90 118 the the DET eurjchem-112 90 119     SPACE eurjchem-112 90 120 catalyst catalyst NOUN eurjchem-112 90 121 , , PUNCT eurjchem-112 90 122     SPACE eurjchem-112 90 123 we we PRON eurjchem-112 90 124     SPACE eurjchem-112 90 125 have have AUX eurjchem-112 90 126     SPACE eurjchem-112 90 127 explored explore VERB eurjchem-112 90 128     SPACE eurjchem-112 90 129 dabco dabco NOUN eurjchem-112 90 130     SPACE eurjchem-112 90 131 as as ADP eurjchem-112 90 132     SPACE eurjchem-112 90 133 a a DET eurjchem-112 90 134     SPACE eurjchem-112 90 135 recyclable recyclable ADJ eurjchem-112 90 136     SPACE eurjchem-112 90 137 catalyst catalyst NOUN eurjchem-112 90 138     SPACE eurjchem-112 90 139 for for ADP eurjchem-112 90 140     SPACE eurjchem-112 90 141 the the DET eurjchem-112 90 142     SPACE eurjchem-112 90 143 synthesis synthesis NOUN eurjchem-112 90 144     SPACE eurjchem-112 90 145 of of ADP eurjchem-112 90 146     SPACE eurjchem-112 90 147 4‐alkyl(aryl)‐3‐cyano‐2(1h)‐iminopyridines 4‐alkyl(aryl)‐3‐cyano‐2(1h)‐iminopyridine NOUN eurjchem-112 90 148     SPACE eurjchem-112 90 149 and and CCONJ eurjchem-112 90 150     SPACE eurjchem-112 90 151 2(1h)‐pyridinones 2(1h)‐pyridinones NUM eurjchem-112 90 152 . . PUNCT eurjchem-112 90 153         SPACE eurjchem-112 91 1 references reference NOUN eurjchem-112 91 2         SPACE eurjchem-112 91 3 [ [ X eurjchem-112 91 4 1 1 NUM eurjchem-112 91 5 ] ] PUNCT eurjchem-112 91 6 . . PUNCT eurjchem-112 92 1 roth roth PROPN eurjchem-112 92 2 , , PUNCT eurjchem-112 92 3     SPACE eurjchem-112 92 4 h. h. PROPN eurjchem-112 92 5     SPACE eurjchem-112 92 6 j. j. PROPN eurjchem-112 92 7 ; ; PUNCT eurjchem-112 92 8     SPACE eurjchem-112 92 9 kleemann kleemann PROPN eurjchem-112 92 10 , , PUNCT eurjchem-112 92 11     SPACE eurjchem-112 92 12 a. a. NOUN eurjchem-112 92 13     SPACE eurjchem-112 92 14 pharmaceutical pharmaceutical NOUN eurjchem-112 92 15     SPACE eurjchem-112 92 16 chemistry chemistry NOUN eurjchem-112 92 17 ; ; PUNCT eurjchem-112 92 18     SPACE eurjchem-112 92 19 eds ed NOUN eurjchem-112 92 20 . . PUNCT eurjchem-112 92 21 ; ; PUNCT eurjchem-112 92 22     SPACE eurjchem-112 92 23 vol vol NOUN eurjchem-112 92 24 . . PUNCT eurjchem-112 92 25     SPACE eurjchem-112 93 1 1 1 NUM eurjchem-112 93 2 : : PUNCT eurjchem-112 93 3     SPACE eurjchem-112 93 4 drug drug NOUN eurjchem-112 93 5     SPACE eurjchem-112 93 6 synthesis synthesis NOUN eurjchem-112 93 7 ; ; PUNCT eurjchem-112 93 8     SPACE eurjchem-112 93 9 john john PROPN eurjchem-112 93 10     SPACE eurjchem-112 93 11 wiley wiley PROPN eurjchem-112 93 12     SPACE eurjchem-112 93 13 & & CCONJ eurjchem-112 93 14     SPACE eurjchem-112 93 15 sons son NOUN eurjchem-112 93 16 : : PUNCT eurjchem-112 93 17     SPACE eurjchem-112 93 18 new new PROPN eurjchem-112 93 19     SPACE eurjchem-112 93 20 york york PROPN eurjchem-112 93 21 , , PUNCT eurjchem-112 93 22     SPACE eurjchem-112 93 23 1988 1988 NUM eurjchem-112 93 24 . . PUNCT eurjchem-112 93 25     SPACE eurjchem-112 94 1 [ [ X eurjchem-112 94 2 2 2 NUM eurjchem-112 94 3 ] ] PUNCT eurjchem-112 94 4 . . PUNCT eurjchem-112 95 1 doe doe NOUN eurjchem-112 95 2 , , PUNCT eurjchem-112 95 3     SPACE eurjchem-112 95 4 k. k. PROPN eurjchem-112 95 5 ; ; PUNCT eurjchem-112 95 6     SPACE eurjchem-112 95 7 avasthi avasthi NOUN eurjchem-112 95 8 , , PUNCT eurjchem-112 95 9     SPACE eurjchem-112 95 10 k. k. PROPN eurjchem-112 95 11 ; ; PUNCT eurjchem-112 95 12     SPACE eurjchem-112 95 13 pratap pratap NOUN eurjchem-112 95 14 , , PUNCT eurjchem-112 95 15     SPACE eurjchem-112 95 16 r. r. PROPN eurjchem-112 95 17 ; ; PUNCT eurjchem-112 95 18     SPACE eurjchem-112 95 19 bakuni bakuni NOUN eurjchem-112 95 20 , , PUNCT eurjchem-112 95 21     SPACE eurjchem-112 95 22 d. d. PROPN eurjchem-112 95 23     SPACE eurjchem-112 95 24 s. s. PROPN eurjchem-112 95 25 ; ; PUNCT eurjchem-112 95 26     SPACE eurjchem-112 95 27 joshi joshi PROPN eurjchem-112 95 28 , , PUNCT eurjchem-112 95 29     SPACE eurjchem-112 95 30 m. m. NOUN eurjchem-112 95 31     SPACE eurjchem-112 95 32 n. n. PROPN eurjchem-112 95 33     SPACE eurjchem-112 95 34 indian indian PROPN eurjchem-112 95 35 . . PUNCT eurjchem-112 95 36     SPACE eurjchem-112 96 1 j. j. PROPN eurjchem-112 96 2     SPACE eurjchem-112 96 3 chem chem NOUN eurjchem-112 96 4 . . PUNCT eurjchem-112 96 5     SPACE eurjchem-112 96 6 1990 1990 NUM eurjchem-112 96 7 , , PUNCT eurjchem-112 96 8     SPACE eurjchem-112 96 9 29 29 NUM eurjchem-112 96 10 , , PUNCT eurjchem-112 96 11     SPACE eurjchem-112 96 12 459‐463 459‐463 NUM eurjchem-112 96 13 . . PUNCT eurjchem-112 96 14     SPACE eurjchem-112 97 1 [ [ X eurjchem-112 97 2 3 3 NUM eurjchem-112 97 3 ] ] PUNCT eurjchem-112 97 4 . . PUNCT eurjchem-112 98 1 shishoo shishoo PROPN eurjchem-112 98 2 , , PUNCT eurjchem-112 98 3     SPACE eurjchem-112 98 4 c. c. PROPN eurjchem-112 98 5     SPACE eurjchem-112 98 6 j. j. PROPN eurjchem-112 98 7 ; ; PUNCT eurjchem-112 98 8     SPACE eurjchem-112 98 9 devani devani ADJ eurjchem-112 98 10 , , PUNCT eurjchem-112 98 11     SPACE eurjchem-112 98 12 m. m. NOUN eurjchem-112 98 13     SPACE eurjchem-112 98 14 b. b. PROPN eurjchem-112 98 15 ; ; PUNCT eurjchem-112 98 16     SPACE eurjchem-112 98 17 bhadti bhadti NOUN eurjchem-112 98 18 , , PUNCT eurjchem-112 98 19     SPACE eurjchem-112 98 20 v. v. ADP eurjchem-112 98 21     SPACE eurjchem-112 98 22 s. s. PROPN eurjchem-112 98 23 ; ; PUNCT eurjchem-112 98 24     SPACE eurjchem-112 98 25 ananthan ananthan ADV eurjchem-112 98 26 , , PUNCT eurjchem-112 98 27     SPACE eurjchem-112 98 28 s. s. PROPN eurjchem-112 98 29 ; ; PUNCT eurjchem-112 98 30     SPACE eurjchem-112 98 31 ullas ulla NOUN eurjchem-112 98 32 , , PUNCT eurjchem-112 98 33     SPACE eurjchem-112 98 34 g. g. PROPN eurjchem-112 98 35     SPACE eurjchem-112 98 36 v. v. PROPN eurjchem-112 98 37       SPACE eurjchem-112 98 38 tetrahedron tetrahedron NOUN eurjchem-112 98 39     SPACE eurjchem-112 98 40 lett lett PROPN eurjchem-112 98 41 . . PUNCT eurjchem-112 98 42     SPACE eurjchem-112 98 43 1983 1983 NUM eurjchem-112 98 44 , , PUNCT eurjchem-112 98 45     SPACE eurjchem-112 98 46 24 24 NUM eurjchem-112 98 47 , , PUNCT eurjchem-112 98 48     SPACE eurjchem-112 98 49 4611‐4612 4611‐4612 NOUN eurjchem-112 98 50 . . PUNCT eurjchem-112 98 51     SPACE eurjchem-112 99 1 [ [ X eurjchem-112 99 2 4 4 NUM eurjchem-112 99 3 ] ] PUNCT eurjchem-112 99 4 . . PUNCT eurjchem-112 100 1 barili barili NOUN eurjchem-112 100 2 , , PUNCT eurjchem-112 100 3     SPACE eurjchem-112 100 4 p. p. NOUN eurjchem-112 100 5     SPACE eurjchem-112 100 6 l. l. PROPN eurjchem-112 100 7 ; ; PUNCT eurjchem-112 100 8     SPACE eurjchem-112 100 9 biagi biagi NOUN eurjchem-112 100 10 , , PUNCT eurjchem-112 100 11     SPACE eurjchem-112 100 12 g. g. NOUN eurjchem-112 100 13 ; ; PUNCT eurjchem-112 100 14     SPACE eurjchem-112 100 15 livi livi NOUN eurjchem-112 100 16 , , PUNCT eurjchem-112 100 17     SPACE eurjchem-112 100 18 o. o. PROPN eurjchem-112 100 19 ; ; PUNCT eurjchem-112 100 20     SPACE eurjchem-112 100 21 mucci mucci PROPN eurjchem-112 100 22 , , PUNCT eurjchem-112 100 23     SPACE eurjchem-112 100 24 l. l. PROPN eurjchem-112 100 25 ; ; PUNCT eurjchem-112 100 26     SPACE eurjchem-112 100 27 scartoni scartoni ADJ eurjchem-112 100 28 , , PUNCT eurjchem-112 100 29     SPACE eurjchem-112 100 30 v. v. ADP eurjchem-112 100 31     SPACE eurjchem-112 100 32 j. j. PROPN eurjchem-112 100 33     SPACE eurjchem-112 100 34 heterocycl heterocycl PROPN eurjchem-112 100 35 . . PUNCT eurjchem-112 100 36     SPACE eurjchem-112 100 37 chem chem NOUN eurjchem-112 100 38 . . PUNCT eurjchem-112 100 39     SPACE eurjchem-112 100 40 1987 1987 NUM eurjchem-112 100 41 , , PUNCT eurjchem-112 100 42     SPACE eurjchem-112 100 43 24 24 NUM eurjchem-112 100 44 , , PUNCT eurjchem-112 100 45     SPACE eurjchem-112 100 46 997‐1001 997‐1001 NUM eurjchem-112 100 47 . . PUNCT eurjchem-112 100 48     SPACE eurjchem-112 101 1 [ [ X eurjchem-112 101 2 5 5 NUM eurjchem-112 101 3 ] ] PUNCT eurjchem-112 101 4 . . PUNCT eurjchem-112 101 5 attia attia PROPN eurjchem-112 101 6 , , PUNCT eurjchem-112 101 7     SPACE eurjchem-112 101 8 a. a. NOUN eurjchem-112 101 9 ; ; PUNCT eurjchem-112 101 10     SPACE eurjchem-112 101 11 michael michael PROPN eurjchem-112 101 12 , , PUNCT eurjchem-112 101 13     SPACE eurjchem-112 101 14 m. m. NOUN eurjchem-112 101 15     SPACE eurjchem-112 101 16 pharmazie pharmazie PROPN eurjchem-112 101 17 . . PUNCT eurjchem-112 101 18     SPACE eurjchem-112 101 19 1982 1982 NUM eurjchem-112 101 20 , , PUNCT eurjchem-112 101 21     SPACE eurjchem-112 101 22 37 37 NUM eurjchem-112 101 23 , , PUNCT eurjchem-112 101 24     SPACE eurjchem-112 101 25 551‐553 551‐553 NUM eurjchem-112 101 26 . . PUNCT eurjchem-112 101 27     SPACE eurjchem-112 102 1 [ [ X eurjchem-112 102 2 6 6 NUM eurjchem-112 102 3 ] ] PUNCT eurjchem-112 102 4 . . PUNCT eurjchem-112 103 1 kambe kambe ADJ eurjchem-112 103 2 , , PUNCT eurjchem-112 103 3     SPACE eurjchem-112 103 4 s. s. PROPN eurjchem-112 103 5 ; ; PUNCT eurjchem-112 103 6     SPACE eurjchem-112 103 7 saito saito ADJ eurjchem-112 103 8 , , PUNCT eurjchem-112 103 9     SPACE eurjchem-112 103 10 k. k. NOUN eurjchem-112 103 11     SPACE eurjchem-112 103 12 synthesis synthesis NOUN eurjchem-112 103 13 . . PUNCT eurjchem-112 103 14     SPACE eurjchem-112 104 1 1980 1980 NUM eurjchem-112 104 2 , , PUNCT eurjchem-112 104 3     SPACE eurjchem-112 104 4 5 5 NUM eurjchem-112 104 5 , , PUNCT eurjchem-112 104 6     SPACE eurjchem-112 104 7 365‐368 365‐368 PROPN eurjchem-112 104 8 . . PUNCT eurjchem-112 104 9     SPACE eurjchem-112 105 1 [ [ X eurjchem-112 105 2 7 7 NUM eurjchem-112 105 3 ] ] PUNCT eurjchem-112 105 4 . . PUNCT eurjchem-112 106 1 domling domling NOUN eurjchem-112 106 2 , , PUNCT eurjchem-112 106 3     SPACE eurjchem-112 106 4 a. a. NOUN eurjchem-112 106 5 ; ; PUNCT eurjchem-112 106 6     SPACE eurjchem-112 106 7 ugi ugi PROPN eurjchem-112 106 8 , , PUNCT eurjchem-112 106 9     SPACE eurjchem-112 106 10 i. i. NOUN eurjchem-112 106 11     SPACE eurjchem-112 106 12 angew angew PROPN eurjchem-112 106 13 . . PUNCT eurjchem-112 106 14     SPACE eurjchem-112 107 1 chem chem NOUN eurjchem-112 107 2 . . PUNCT eurjchem-112 107 3     SPACE eurjchem-112 108 1 int int NOUN eurjchem-112 108 2 . . PUNCT eurjchem-112 108 3     SPACE eurjchem-112 109 1 ed ed NOUN eurjchem-112 109 2 . . PUNCT eurjchem-112 109 3     SPACE eurjchem-112 110 1 2000 2000 NUM eurjchem-112 110 2 , , PUNCT eurjchem-112 110 3     SPACE eurjchem-112 110 4 39 39 NUM eurjchem-112 110 5 , , PUNCT eurjchem-112 110 6     SPACE eurjchem-112 110 7 3168‐3210 3168‐3210 NUM eurjchem-112 110 8 . . PUNCT eurjchem-112 110 9     SPACE eurjchem-112 111 1 [ [ X eurjchem-112 111 2 8 8 NUM eurjchem-112 111 3 ] ] PUNCT eurjchem-112 111 4 . . PUNCT eurjchem-112 112 1 domling domling NOUN eurjchem-112 112 2 , , PUNCT eurjchem-112 112 3     SPACE eurjchem-112 112 4 a. a. NOUN eurjchem-112 112 5     SPACE eurjchem-112 112 6 comb comb NOUN eurjchem-112 112 7 . . PUNCT eurjchem-112 112 8     SPACE eurjchem-112 112 9 chem chem NOUN eurjchem-112 112 10 . . PUNCT eurjchem-112 112 11     SPACE eurjchem-112 112 12 1998 1998 NUM eurjchem-112 112 13 , , PUNCT eurjchem-112 112 14     SPACE eurjchem-112 112 15 1 1 NUM eurjchem-112 112 16 , , PUNCT eurjchem-112 112 17     SPACE eurjchem-112 112 18 1‐22 1‐22 NUM eurjchem-112 112 19 . . PUNCT eurjchem-112 112 20     SPACE eurjchem-112 113 1 [ [ X eurjchem-112 113 2 9 9 NUM eurjchem-112 113 3 ] ] PUNCT eurjchem-112 113 4 . . PUNCT eurjchem-112 114 1 pan pan PROPN eurjchem-112 114 2 . . PROPN eurjchem-112 114 3     SPACE eurjchem-112 114 4 j. j. PROPN eurjchem-112 114 5     SPACE eurjchem-112 114 6 f. f. PROPN eurjchem-112 114 7 ; ; PUNCT eurjchem-112 114 8         SPACE eurjchem-112 114 9 chen chen PROPN eurjchem-112 114 10 , , PUNCT eurjchem-112 114 11     SPACE eurjchem-112 114 12 k. k. PROPN eurjchem-112 114 13     SPACE eurjchem-112 114 14 tetrahedron tetrahedron NOUN eurjchem-112 114 15     SPACE eurjchem-112 114 16 lett lett PROPN eurjchem-112 114 17 . . PUNCT eurjchem-112 114 18     SPACE eurjchem-112 114 19 2004 2004 NUM eurjchem-112 114 20 , , PUNCT eurjchem-112 114 21     SPACE eurjchem-112 114 22 45 45 NUM eurjchem-112 114 23 , , PUNCT eurjchem-112 114 24     SPACE eurjchem-112 114 25 2541‐2543 2541‐2543 NUM eurjchem-112 114 26 . . PUNCT eurjchem-112 114 27     SPACE eurjchem-112 115 1 [ [ X eurjchem-112 115 2 10 10 NUM eurjchem-112 115 3 ] ] PUNCT eurjchem-112 115 4 . . PUNCT eurjchem-112 116 1 sheen sheen PROPN eurjchem-112 116 2 , , PUNCT eurjchem-112 116 3     SPACE eurjchem-112 116 4 w. w. PROPN eurjchem-112 116 5     SPACE eurjchem-112 116 6 c. c. PROPN eurjchem-112 116 7 ; ; PUNCT eurjchem-112 116 8     SPACE eurjchem-112 116 9 lazanov lazanov NOUN eurjchem-112 116 10 , , PUNCT eurjchem-112 116 11     SPACE eurjchem-112 116 12 m. m. NOUN eurjchem-112 116 13     SPACE eurjchem-112 116 14 ; ; PUNCT eurjchem-112 116 15       SPACE eurjchem-112 116 16 rejic rejic ADJ eurjchem-112 116 17 , , PUNCT eurjchem-112 116 18     SPACE eurjchem-112 116 19 o. o. PROPN eurjchem-112 116 20     SPACE eurjchem-112 116 21 tetrahedron tetrahedron NOUN eurjchem-112 116 22     SPACE eurjchem-112 116 23 lett lett PROPN eurjchem-112 116 24 . . PUNCT eurjchem-112 116 25     SPACE eurjchem-112 116 26 2003 2003 NUM eurjchem-112 116 27 , , PUNCT eurjchem-112 116 28     SPACE eurjchem-112 116 29 44 44 NUM eurjchem-112 116 30 , , PUNCT eurjchem-112 116 31     SPACE eurjchem-112 116 32 6943‐ 6943‐ NUM eurjchem-112 116 33 6945 6945 NUM eurjchem-112 116 34 . . PUNCT eurjchem-112 116 35         SPACE eurjchem-112 117 1 [ [ X eurjchem-112 117 2 11 11 NUM eurjchem-112 117 3 ] ] PUNCT eurjchem-112 117 4 . . PUNCT eurjchem-112 118 1 takkewaki takkewaki NOUN eurjchem-112 118 2 , , PUNCT eurjchem-112 118 3     SPACE eurjchem-112 118 4 t. t. PROPN eurjchem-112 118 5 ; ; PUNCT eurjchem-112 118 6     SPACE eurjchem-112 118 7 beck beck NOUN eurjchem-112 118 8 , , PUNCT eurjchem-112 118 9     SPACE eurjchem-112 118 10 l. l. PROPN eurjchem-112 118 11     SPACE eurjchem-112 118 12 w. w. PROPN eurjchem-112 118 13 ; ; PUNCT eurjchem-112 118 14     SPACE eurjchem-112 118 15 danis danis NOUN eurjchem-112 118 16 , , PUNCT eurjchem-112 118 17     SPACE eurjchem-112 118 18 m. m. NOUN eurjchem-112 118 19     SPACE eurjchem-112 118 20 e. e. PROPN eurjchem-112 118 21     SPACE eurjchem-112 118 22 micropor micropor PROPN eurjchem-112 118 23 . . PUNCT eurjchem-112 118 24     SPACE eurjchem-112 118 25 mesopor mesopor PROPN eurjchem-112 118 26 . . PUNCT eurjchem-112 118 27     SPACE eurjchem-112 118 28 mater mater NOUN eurjchem-112 118 29 . . PUNCT eurjchem-112 118 30     SPACE eurjchem-112 118 31 1999 1999 NUM eurjchem-112 118 32 , , PUNCT eurjchem-112 118 33     SPACE eurjchem-112 118 34 33 33 NUM eurjchem-112 118 35 , , PUNCT eurjchem-112 118 36     SPACE eurjchem-112 118 37 197‐207 197‐207 NOUN eurjchem-112 118 38 . . PUNCT eurjchem-112 118 39     SPACE eurjchem-112 119 1 [ [ X eurjchem-112 119 2 12 12 NUM eurjchem-112 119 3 ] ] PUNCT eurjchem-112 119 4 . . PUNCT eurjchem-112 120 1 veeraraghavan veeraraghavan PROPN eurjchem-112 120 2 , , PUNCT eurjchem-112 120 3     SPACE eurjchem-112 120 4 p. p. NOUN eurjchem-112 120 5 ; ; PUNCT eurjchem-112 120 6     SPACE eurjchem-112 120 7 michael michael PROPN eurjchem-112 120 8 , , PUNCT eurjchem-112 120 9     SPACE eurjchem-112 120 10 r. r. PROPN eurjchem-112 120 11 ; ; PUNCT eurjchem-112 120 12     SPACE eurjchem-112 120 13 rudd rudd PROPN eurjchem-112 120 14 , , PUNCT eurjchem-112 120 15     SPACE eurjchem-112 120 16 t. t. PROPN eurjchem-112 120 17 ; ; PUNCT eurjchem-112 120 18     SPACE eurjchem-112 120 19 reddy reddy NOUN eurjchem-112 120 20 , , PUNCT eurjchem-112 120 21     SPACE eurjchem-112 120 22 m. m. NOUN eurjchem-112 120 23     SPACE eurjchem-112 120 24 v. v. PROPN eurjchem-112 120 25     SPACE eurjchem-112 120 26 r. r. PROPN eurjchem-112 120 27     SPACE eurjchem-112 120 28 tetrahedron tetrahedron PROPN eurjchem-112 120 29     SPACE eurjchem-112 120 30 lett lett NOUN eurjchem-112 120 31 . . PUNCT eurjchem-112 120 32     SPACE eurjchem-112 120 33 1999 1999 NUM eurjchem-112 120 34 , , PUNCT eurjchem-112 120 35     SPACE eurjchem-112 120 36 40 40 NUM eurjchem-112 120 37 , , PUNCT eurjchem-112 120 38     SPACE eurjchem-112 120 39 3819‐3822 3819‐3822 NUM eurjchem-112 120 40 . . PUNCT eurjchem-112 120 41     SPACE eurjchem-112 121 1 [ [ X eurjchem-112 121 2 13 13 NUM eurjchem-112 121 3 ] ] PUNCT eurjchem-112 121 4 . . PUNCT eurjchem-112 122 1 basavaiah basavaiah PROPN eurjchem-112 122 2 , , PUNCT eurjchem-112 122 3     SPACE eurjchem-112 122 4 d. d. PROPN eurjchem-112 122 5 ; ; PUNCT eurjchem-112 122 6     SPACE eurjchem-112 122 7 bharathi bharathi NOUN eurjchem-112 122 8 , , PUNCT eurjchem-112 122 9     SPACE eurjchem-112 122 10 t. t. PROPN eurjchem-112 122 11     SPACE eurjchem-112 122 12 k. k. PROPN eurjchem-112 122 13     SPACE eurjchem-112 122 14 ; ; PUNCT eurjchem-112 122 15     SPACE eurjchem-112 122 16 gawzeswaie gawzeswaie NOUN eurjchem-112 122 17 , , PUNCT eurjchem-112 122 18     SPACE eurjchem-112 122 19 v. v. NOUN eurjchem-112 122 20     SPACE eurjchem-112 122 21 v. v. ADP eurjchem-112 122 22     SPACE eurjchem-112 122 23 l. l. PROPN eurjchem-112 122 24     SPACE eurjchem-112 122 25 tetrahedron tetrahedron PROPN eurjchem-112 122 26     SPACE eurjchem-112 122 27 lett lett PROPN eurjchem-112 122 28 . . PUNCT eurjchem-112 122 29     SPACE eurjchem-112 122 30 1987 1987 NUM eurjchem-112 122 31 , , PUNCT eurjchem-112 122 32     SPACE eurjchem-112 122 33 28 28 NUM eurjchem-112 122 34 , , PUNCT eurjchem-112 122 35     SPACE eurjchem-112 122 36 4352‐4651 4352‐4651 NUM eurjchem-112 122 37 . . PUNCT eurjchem-112 122 38     SPACE eurjchem-112 123 1 [ [ X eurjchem-112 123 2 14 14 NUM eurjchem-112 123 3 ] ] PUNCT eurjchem-112 123 4 . . PUNCT eurjchem-112 124 1 basavaiah basavaiah PROPN eurjchem-112 124 2 , , PUNCT eurjchem-112 124 3     SPACE eurjchem-112 124 4 d. d. PROPN eurjchem-112 124 5 ; ; PUNCT eurjchem-112 124 6     SPACE eurjchem-112 124 7 gawriswari gawriswari PROPN eurjchem-112 124 8 ; ; PUNCT eurjchem-112 124 9     SPACE eurjchem-112 124 10 v. v. NOUN eurjchem-112 124 11     SPACE eurjchem-112 124 12 v. v. NOUN eurjchem-112 124 13     SPACE eurjchem-112 124 14 l. l. PROPN eurjchem-112 124 15 ; ; PUNCT eurjchem-112 124 16     SPACE eurjchem-112 124 17 baharathine baharathine NOUN eurjchem-112 124 18 , , PUNCT eurjchem-112 124 19     SPACE eurjchem-112 124 20 t. t. PROPN eurjchem-112 124 21     SPACE eurjchem-112 124 22 k. k. PROPN eurjchem-112 124 23     SPACE eurjchem-112 124 24 tetrahedron tetrahedron NOUN eurjchem-112 124 25     SPACE eurjchem-112 124 26 lett lett PROPN eurjchem-112 124 27 . . PUNCT eurjchem-112 124 28     SPACE eurjchem-112 124 29 1987 1987 NUM eurjchem-112 124 30 , , PUNCT eurjchem-112 124 31     SPACE eurjchem-112 124 32 28 28 NUM eurjchem-112 124 33 , , PUNCT eurjchem-112 124 34     SPACE eurjchem-112 124 35 4591‐4592 4591‐4592 NUM eurjchem-112 124 36 . . PUNCT eurjchem-112 124 37     SPACE eurjchem-112 125 1 [ [ X eurjchem-112 125 2 15 15 NUM eurjchem-112 125 3 ] ] PUNCT eurjchem-112 125 4 . . PUNCT eurjchem-112 126 1 bamoharram bamoharram PROPN eurjchem-112 126 2 , , PUNCT eurjchem-112 126 3     SPACE eurjchem-112 126 4 f. f. PROPN eurjchem-112 126 5     SPACE eurjchem-112 126 6 f. f. PROPN eurjchem-112 126 7 ; ; PUNCT eurjchem-112 126 8     SPACE eurjchem-112 126 9 heravi heravi NOUN eurjchem-112 126 10 , , PUNCT eurjchem-112 126 11     SPACE eurjchem-112 126 12 m. m. NOUN eurjchem-112 126 13     SPACE eurjchem-112 126 14 m. m. NOUN eurjchem-112 126 15 ; ; PUNCT eurjchem-112 126 16     SPACE eurjchem-112 126 17 roshani roshani NOUN eurjchem-112 126 18 , , PUNCT eurjchem-112 126 19     SPACE eurjchem-112 126 20 m. m. NOUN eurjchem-112 126 21 ; ; PUNCT eurjchem-112 126 22     SPACE eurjchem-112 126 23 gharib gharib PROPN eurjchem-112 126 24 , , PUNCT eurjchem-112 126 25     SPACE eurjchem-112 126 26 a. a. NOUN eurjchem-112 126 27 ; ; PUNCT eurjchem-112 126 28     SPACE eurjchem-112 126 29 jahangir jahangir PROPN eurjchem-112 126 30 , , PUNCT eurjchem-112 126 31     SPACE eurjchem-112 126 32 m. m. NOUN eurjchem-112 126 33     SPACE eurjchem-112 126 34 appl appl PROPN eurjchem-112 126 35 . . PUNCT eurjchem-112 126 36     SPACE eurjchem-112 126 37 catal catal NOUN eurjchem-112 126 38 . . PUNCT eurjchem-112 126 39     SPACE eurjchem-112 126 40 2006 2006 NUM eurjchem-112 126 41 , , PUNCT eurjchem-112 126 42     SPACE eurjchem-112 126 43 302 302 NUM eurjchem-112 126 44 , , PUNCT eurjchem-112 126 45     SPACE eurjchem-112 126 46 42‐47 42‐47 NOUN eurjchem-112 126 47 . . PUNCT eurjchem-112 126 48       SPACE eurjchem-112 127 1 [ [ X eurjchem-112 127 2 16 16 NUM eurjchem-112 127 3 ] ] PUNCT eurjchem-112 127 4 . . PUNCT eurjchem-112 128 1 heravi heravi PROPN eurjchem-112 128 2 , , PUNCT eurjchem-112 128 3     SPACE eurjchem-112 128 4 m. m. NOUN eurjchem-112 128 5     SPACE eurjchem-112 128 6 m. m. NOUN eurjchem-112 128 7 ; ; PUNCT eurjchem-112 128 8         SPACE eurjchem-112 128 9 hekmatshoar hekmatshoar NOUN eurjchem-112 128 10 , , PUNCT eurjchem-112 128 11     SPACE eurjchem-112 128 12 r. r. PROPN eurjchem-112 128 13 ; ; PUNCT eurjchem-112 128 14     SPACE eurjchem-112 128 15 pedram pedram NOUN eurjchem-112 128 16 , , PUNCT eurjchem-112 128 17     SPACE eurjchem-112 128 18 l. l. PROPN eurjchem-112 128 19     SPACE eurjchem-112 128 20 j. j. PROPN eurjchem-112 128 21     SPACE eurjchem-112 128 22 mol mol PROPN eurjchem-112 128 23 . . PROPN eurjchem-112 128 24     SPACE eurjchem-112 128 25 catal catal NOUN eurjchem-112 128 26 . . PUNCT eurjchem-112 128 27     SPACE eurjchem-112 128 28 a. a. NOUN eurjchem-112 128 29     SPACE eurjchem-112 128 30 chem chem NOUN eurjchem-112 128 31 . . PUNCT eurjchem-112 128 32     SPACE eurjchem-112 128 33 2005 2005 NUM eurjchem-112 128 34 , , PUNCT eurjchem-112 128 35     SPACE eurjchem-112 128 36 231 231 NUM eurjchem-112 128 37 , , PUNCT eurjchem-112 128 38     SPACE eurjchem-112 128 39 89‐91 89‐91 NOUN eurjchem-112 128 40 . . PUNCT eurjchem-112 128 41     SPACE eurjchem-112 129 1 [ [ X eurjchem-112 129 2 17 17 NUM eurjchem-112 129 3 ] ] PUNCT eurjchem-112 129 4 . . PUNCT eurjchem-112 130 1 heravi heravi PROPN eurjchem-112 130 2 , , PUNCT eurjchem-112 130 3     SPACE eurjchem-112 130 4 m. m. NOUN eurjchem-112 130 5     SPACE eurjchem-112 130 6 m. m. NOUN eurjchem-112 130 7 ; ; PUNCT eurjchem-112 130 8     SPACE eurjchem-112 130 9 bakhtiari bakhtiari ADJ eurjchem-112 130 10 , , PUNCT eurjchem-112 130 11     SPACE eurjchem-112 130 12 k. k. PROPN eurjchem-112 130 13 ; ; PUNCT eurjchem-112 130 14     SPACE eurjchem-112 130 15 oskooie oskooie NOUN eurjchem-112 130 16 , , PUNCT eurjchem-112 130 17     SPACE eurjchem-112 130 18 h. h. PROPN eurjchem-112 130 19     SPACE eurjchem-112 130 20 a. a. PROPN eurjchem-112 130 21     SPACE eurjchem-112 130 22 j. j. PROPN eurjchem-112 130 23     SPACE eurjchem-112 130 24 chin chin PROPN eurjchem-112 130 25 . . PUNCT eurjchem-112 130 26     SPACE eurjchem-112 130 27 chem chem NOUN eurjchem-112 130 28 . . PUNCT eurjchem-112 130 29     SPACE eurjchem-112 130 30 soc soc PROPN eurjchem-112 130 31 . . PUNCT eurjchem-112 130 32     SPACE eurjchem-112 131 1 2007 2007 NUM eurjchem-112 131 2 , , PUNCT eurjchem-112 131 3     SPACE eurjchem-112 131 4 54 54 NUM eurjchem-112 131 5 , , PUNCT eurjchem-112 131 6     SPACE eurjchem-112 131 7 579‐581 579‐581 NOUN eurjchem-112 131 8 . . PUNCT eurjchem-112 131 9     SPACE eurjchem-112 132 1 [ [ X eurjchem-112 132 2 18 18 NUM eurjchem-112 132 3 ] ] PUNCT eurjchem-112 132 4 . . PUNCT eurjchem-112 132 5 heravi heravi PROPN eurjchem-112 132 6 , , PUNCT eurjchem-112 132 7     SPACE eurjchem-112 132 8 m. m. NOUN eurjchem-112 132 9     SPACE eurjchem-112 132 10 m. m. NOUN eurjchem-112 132 11 ; ; PUNCT eurjchem-112 132 12     SPACE eurjchem-112 132 13 oskooie oskooie NOUN eurjchem-112 132 14 , , PUNCT eurjchem-112 132 15     SPACE eurjchem-112 132 16 h. h. PROPN eurjchem-112 132 17     SPACE eurjchem-112 132 18 a. a. NOUN eurjchem-112 132 19 ; ; PUNCT eurjchem-112 132 20     SPACE eurjchem-112 132 21 baghernejad baghernejad NOUN eurjchem-112 132 22 , , PUNCT eurjchem-112 132 23     SPACE eurjchem-112 132 24 b. b. PROPN eurjchem-112 132 25     SPACE eurjchem-112 132 26 j. j. PROPN eurjchem-112 132 27     SPACE eurjchem-112 132 28 chin chin PROPN eurjchem-112 132 29 . . PUNCT eurjchem-112 132 30     SPACE eurjchem-112 132 31 chem chem NOUN eurjchem-112 132 32 . . PUNCT eurjchem-112 132 33     SPACE eurjchem-112 132 34 soc soc PROPN eurjchem-112 132 35 . . PUNCT eurjchem-112 132 36     SPACE eurjchem-112 132 37 2007 2007 NUM eurjchem-112 132 38 , , PUNCT eurjchem-112 132 39     SPACE eurjchem-112 132 40 54 54 NUM eurjchem-112 132 41 , , PUNCT eurjchem-112 132 42     SPACE eurjchem-112 132 43 767‐770 767‐770 NOUN eurjchem-112 132 44 . . PUNCT eurjchem-112 132 45     SPACE eurjchem-112 133 1 [ [ X eurjchem-112 133 2 19 19 NUM eurjchem-112 133 3 ] ] PUNCT eurjchem-112 133 4 . . PUNCT eurjchem-112 134 1 lin lin PROPN eurjchem-112 134 2 , , PUNCT eurjchem-112 134 3     SPACE eurjchem-112 134 4 x. x. NOUN eurjchem-112 134 5 ; ; PUNCT eurjchem-112 134 6     SPACE eurjchem-112 134 7 poeppelmeier poeppelmeier NOUN eurjchem-112 134 8 , , PUNCT eurjchem-112 134 9     SPACE eurjchem-112 134 10 k. k. PROPN eurjchem-112 134 11     SPACE eurjchem-112 134 12 r. r. PROPN eurjchem-112 134 13 ; ; PUNCT eurjchem-112 134 14     SPACE eurjchem-112 134 15 weitz weitz PROPN eurjchem-112 134 16 , , PUNCT eurjchem-112 134 17     SPACE eurjchem-112 134 18 e. e. PROPN eurjchem-112 134 19     SPACE eurjchem-112 134 20 appl appl PROPN eurjchem-112 134 21 . . PUNCT eurjchem-112 134 22     SPACE eurjchem-112 134 23 catal catal NOUN eurjchem-112 134 24 . . PUNCT eurjchem-112 134 25     SPACE eurjchem-112 135 1 a a DET eurjchem-112 135 2 : : PUNCT eurjchem-112 135 3     SPACE eurjchem-112 135 4 gen gen PROPN eurjchem-112 135 5 . . PROPN eurjchem-112 135 6     SPACE eurjchem-112 135 7 2010 2010 NUM eurjchem-112 135 8 , , PUNCT eurjchem-112 135 9     SPACE eurjchem-112 135 10 381 381 NUM eurjchem-112 135 11 , , PUNCT eurjchem-112 135 12     SPACE eurjchem-112 135 13 114‐120 114‐120 NUM eurjchem-112 135 14 . . PUNCT eurjchem-112 135 15     SPACE eurjchem-112 136 1 [ [ X eurjchem-112 136 2 20 20 NUM eurjchem-112 136 3 ] ] PUNCT eurjchem-112 136 4 . . PUNCT eurjchem-112 137 1 abadi abadi PROPN eurjchem-112 137 2 , , PUNCT eurjchem-112 137 3     SPACE eurjchem-112 137 4 a. a. NOUN eurjchem-112 137 5 ; ; PUNCT eurjchem-112 137 6     SPACE eurjchem-112 137 7 al‐deeb al‐deeb PROPN eurjchem-112 137 8 , , PUNCT eurjchem-112 137 9     SPACE eurjchem-112 137 10 o. o. PROPN eurjchem-112 137 11 ; ; PUNCT eurjchem-112 137 12     SPACE eurjchem-112 137 13 al‐afify al‐afify VERB eurjchem-112 137 14 , , PUNCT eurjchem-112 137 15     SPACE eurjchem-112 137 16 a. a. NOUN eurjchem-112 137 17 ; ; PUNCT eurjchem-112 137 18     SPACE eurjchem-112 137 19 el‐kashef el‐kashef PROPN eurjchem-112 137 20 , , PUNCT eurjchem-112 137 21     SPACE eurjchem-112 137 22 h. h. PROPN eurjchem-112 137 23     SPACE eurjchem-112 137 24 farmaco farmaco PROPN eurjchem-112 137 25     SPACE eurjchem-112 137 26 ii ii NOUN eurjchem-112 137 27     SPACE eurjchem-112 137 28 1999 1999 NUM eurjchem-112 137 29 , , PUNCT eurjchem-112 137 30     SPACE eurjchem-112 137 31 54 54 NUM eurjchem-112 137 32 , , PUNCT eurjchem-112 137 33     SPACE eurjchem-112 137 34 195‐201 195‐201 NUM eurjchem-112 137 35 . . PUNCT eurjchem-112 137 36     SPACE eurjchem-112 138 1 [ [ X eurjchem-112 138 2 21 21 NUM eurjchem-112 138 3 ] ] PUNCT eurjchem-112 138 4 . . PUNCT eurjchem-112 138 5 heravi heravi PROPN eurjchem-112 138 6 , , PUNCT eurjchem-112 138 7     SPACE eurjchem-112 138 8 m. m. NOUN eurjchem-112 138 9     SPACE eurjchem-112 138 10 m. m. NOUN eurjchem-112 138 11 ; ; PUNCT eurjchem-112 138 12     SPACE eurjchem-112 138 13 beheshtia beheshtia NOUN eurjchem-112 138 14 , , PUNCT eurjchem-112 138 15     SPACE eurjchem-112 138 16 y. y. NOUN eurjchem-112 138 17     SPACE eurjchem-112 138 18 s. s. PROPN eurjchem-112 138 19 ; ; PUNCT eurjchem-112 138 20     SPACE eurjchem-112 138 21 khorshidi khorshidi NOUN eurjchem-112 138 22 , , PUNCT eurjchem-112 138 23     SPACE eurjchem-112 138 24 m. m. NOUN eurjchem-112 138 25 ; ; PUNCT eurjchem-112 138 26     SPACE eurjchem-112 138 27 baghernejad baghernejad NOUN eurjchem-112 138 28 , , PUNCT eurjchem-112 138 29     SPACE eurjchem-112 138 30 b. b. PROPN eurjchem-112 138 31 ; ; PUNCT eurjchem-112 138 32     SPACE eurjchem-112 138 33 bamoharram bamoharram NOUN eurjchem-112 138 34 , , PUNCT eurjchem-112 138 35     SPACE eurjchem-112 138 36 f. f. PROPN eurjchem-112 138 37     SPACE eurjchem-112 138 38 chin chin PROPN eurjchem-112 138 39 . . PUNCT eurjchem-112 138 40     SPACE eurjchem-112 138 41 j. j. PROPN eurjchem-112 138 42     SPACE eurjchem-112 138 43 chem chem NOUN eurjchem-112 138 44 . . PUNCT eurjchem-112 138 45     SPACE eurjchem-112 139 1 2009 2009 NUM eurjchem-112 139 2 , , PUNCT eurjchem-112 139 3     SPACE eurjchem-112 139 4 27 27 NUM eurjchem-112 139 5 , , PUNCT eurjchem-112 139 6     SPACE eurjchem-112 139 7 569‐572 569‐572 NUM eurjchem-112 139 8 . . PUNCT eurjchem-112 139 9     SPACE