id	sid	tid	token	lemma	pos
eurjchem-1125	1	1	untitled	untitle	VERB
eurjchem-1125	1	2	european	european	PROPN
eurjchem-1125	1	3	journal	journal	PROPN
eurjchem-1125	1	4	of	of	ADP
eurjchem-1125	1	5	chemistry	chemistry	NOUN
eurjchem-1125	1	6	5	5	NUM
eurjchem-1125	1	7	(	(	PUNCT
eurjchem-1125	1	8	4	4	NUM
eurjchem-1125	1	9	)	)	PUNCT
eurjchem-1125	1	10	(	(	PUNCT
eurjchem-1125	1	11	2014	2014	NUM
eurjchem-1125	1	12	)	)	PUNCT
eurjchem-1125	1	13	644‐651	644‐651	ADJ
eurjchem-1125	1	14	european	european	ADJ
eurjchem-1125	1	15	journal	journal	PROPN
eurjchem-1125	1	16	of	of	ADP
eurjchem-1125	1	17	chemistry	chemistry	NOUN
eurjchem-1125	1	18	issn	issn	PROPN
eurjchem-1125	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-1125	1	20	(	(	PUNCT
eurjchem-1125	1	21	print	print	NOUN
eurjchem-1125	1	22	)	)	PUNCT
eurjchem-1125	1	23	/	/	SYM
eurjchem-1125	1	24	issn	issn	PROPN
eurjchem-1125	1	25	2153‐2257	2153‐2257	NUM
eurjchem-1125	1	26	(	(	PUNCT
eurjchem-1125	1	27	online	online	ADJ
eurjchem-1125	1	28	)	)	PUNCT
eurjchem-1125	1	29			NOUN
eurjchem-1125	1	30	2014	2014	NUM
eurjchem-1125	2	1	eurjchem	eurjchem	PROPN
eurjchem-1125	2	2	publishing	publish	VERB
eurjchem-1125	2	3	‐	‐	NOUN
eurjchem-1125	2	4	printed	print	VERB
eurjchem-1125	2	5	in	in	ADP
eurjchem-1125	2	6	the	the	DET
eurjchem-1125	2	7	usa	usa	PROPN
eurjchem-1125	2	8	http://dx.doi.org/10.5155/eurjchem.5.4.644‐651.1125	http://dx.doi.org/10.5155/eurjchem.5.4.644‐651.1125	NUM
eurjchem-1125	2	9	european	european	PROPN
eurjchem-1125	2	10	journal	journal	PROPN
eurjchem-1125	2	11	of	of	ADP
eurjchem-1125	2	12	chemistry	chemistry	PROPN
eurjchem-1125	2	13	journal	journal	PROPN
eurjchem-1125	2	14	homepage	homepage	NOUN
eurjchem-1125	2	15	:	:	PUNCT
eurjchem-1125	2	16	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1125	2	17	synthesis	synthesis	NOUN
eurjchem-1125	2	18	and	and	CCONJ
eurjchem-1125	2	19	antioxidant	antioxidant	ADJ
eurjchem-1125	2	20	evaluation	evaluation	NOUN
eurjchem-1125	2	21	of	of	ADP
eurjchem-1125	2	22	novel	novel	ADJ
eurjchem-1125	2	23	sophisticated	sophisticated	ADJ
eurjchem-1125	2	24	carboxamides	carboxamide	NOUN
eurjchem-1125	2	25	based	base	VERB
eurjchem-1125	2	26	on	on	ADP
eurjchem-1125	2	27	3‐(ethoxycarbonyl)‐4,5,6,7‐tetrahydro‐1‐benzothiophen‐2‐amine	3‐(ethoxycarbonyl)‐4,5,6,7‐tetrahydro‐1‐benzothiophen‐2‐amine	NUM
eurjchem-1125	2	28	moustafa	moustafa	NOUN
eurjchem-1125	2	29	ahmed	ahmed	PROPN
eurjchem-1125	2	30	gouda	gouda	PROPN
eurjchem-1125	2	31	a	a	PROPN
eurjchem-1125	2	32	,	,	PUNCT
eurjchem-1125	2	33	b	b	NOUN
eurjchem-1125	2	34	,	,	PUNCT
eurjchem-1125	2	35	*	*	PUNCT
eurjchem-1125	2	36	and	and	CCONJ
eurjchem-1125	2	37	serry	serry	PROPN
eurjchem-1125	2	38	atta	atta	PROPN
eurjchem-1125	2	39	atta	atta	PROPN
eurjchem-1125	2	40	el	el	PROPN
eurjchem-1125	2	41	bialy	bialy	PROPN
eurjchem-1125	2	42	c	c	PROPN
eurjchem-1125	2	43	a	a	DET
eurjchem-1125	2	44	chemistry	chemistry	NOUN
eurjchem-1125	2	45	department	department	NOUN
eurjchem-1125	2	46	,	,	PUNCT
eurjchem-1125	2	47	faculty	faculty	NOUN
eurjchem-1125	2	48	of	of	ADP
eurjchem-1125	2	49	science	science	NOUN
eurjchem-1125	2	50	,	,	PUNCT
eurjchem-1125	2	51	mansoura	mansoura	PROPN
eurjchem-1125	2	52	university	university	NOUN
eurjchem-1125	2	53	,	,	PUNCT
eurjchem-1125	2	54	mansoura	mansoura	NOUN
eurjchem-1125	2	55	35516	35516	NUM
eurjchem-1125	2	56	,	,	PUNCT
eurjchem-1125	2	57	egypt	egypt	PROPN
eurjchem-1125	2	58	b	b	PROPN
eurjchem-1125	2	59	department	department	PROPN
eurjchem-1125	2	60	of	of	ADP
eurjchem-1125	2	61	chemistry	chemistry	NOUN
eurjchem-1125	2	62	,	,	PUNCT
eurjchem-1125	2	63	faculty	faculty	NOUN
eurjchem-1125	2	64	of	of	ADP
eurjchem-1125	2	65	science	science	NOUN
eurjchem-1125	2	66	and	and	CCONJ
eurjchem-1125	2	67	arts	art	NOUN
eurjchem-1125	2	68	,	,	PUNCT
eurjchem-1125	2	69	taibah	taibah	PROPN
eurjchem-1125	2	70	university	university	PROPN
eurjchem-1125	2	71	,	,	PUNCT
eurjchem-1125	2	72	ulla	ulla	PROPN
eurjchem-1125	2	73	,	,	PUNCT
eurjchem-1125	2	74	41411	41411	NUM
eurjchem-1125	2	75	,	,	PUNCT
eurjchem-1125	2	76	kingdom	kingdom	NOUN
eurjchem-1125	2	77	of	of	ADP
eurjchem-1125	2	78	saudi	saudi	PROPN
eurjchem-1125	2	79	arabia	arabia	PROPN
eurjchem-1125	2	80	c	c	PROPN
eurjchem-1125	2	81	department	department	PROPN
eurjchem-1125	2	82	of	of	ADP
eurjchem-1125	2	83	pharmaceutical	pharmaceutical	ADJ
eurjchem-1125	2	84	organic	organic	ADJ
eurjchem-1125	2	85	chemistry	chemistry	NOUN
eurjchem-1125	2	86	,	,	PUNCT
eurjchem-1125	2	87	faculty	faculty	NOUN
eurjchem-1125	2	88	of	of	ADP
eurjchem-1125	2	89	pharmacy	pharmacy	NOUN
eurjchem-1125	2	90	,	,	PUNCT
eurjchem-1125	2	91	mansoura	mansoura	PROPN
eurjchem-1125	2	92	university	university	NOUN
eurjchem-1125	2	93	,	,	PUNCT
eurjchem-1125	2	94	mansoura	mansoura	NOUN
eurjchem-1125	2	95	35516	35516	NUM
eurjchem-1125	2	96	,	,	PUNCT
eurjchem-1125	2	97	egypt	egypt	PROPN
eurjchem-1125	2	98	*	*	PUNCT
eurjchem-1125	2	99	corresponding	correspond	VERB
eurjchem-1125	2	100	author	author	NOUN
eurjchem-1125	2	101	at	at	ADP
eurjchem-1125	2	102	:	:	PUNCT
eurjchem-1125	2	103	chemistry	chemistry	NOUN
eurjchem-1125	2	104	department	department	NOUN
eurjchem-1125	2	105	,	,	PUNCT
eurjchem-1125	2	106	faculty	faculty	NOUN
eurjchem-1125	2	107	of	of	ADP
eurjchem-1125	2	108	science	science	NOUN
eurjchem-1125	2	109	,	,	PUNCT
eurjchem-1125	2	110	mansoura	mansoura	PROPN
eurjchem-1125	2	111	university	university	NOUN
eurjchem-1125	2	112	,	,	PUNCT
eurjchem-1125	2	113	mansoura	mansoura	PROPN
eurjchem-1125	2	114	35516	35516	NUM
eurjchem-1125	2	115	,	,	PUNCT
eurjchem-1125	2	116	egypt	egypt	PROPN
eurjchem-1125	2	117	.	.	PUNCT
eurjchem-1125	3	1	tel	tel	PROPN
eurjchem-1125	3	2	.	.	PUNCT
eurjchem-1125	3	3	:	:	PUNCT
eurjchem-1125	4	1	+2.050.6432235	+2.050.6432235	ADJ
eurjchem-1125	4	2	.	.	PUNCT
eurjchem-1125	4	3	fax	fax	NOUN
eurjchem-1125	4	4	:	:	PUNCT
eurjchem-1125	4	5	+2.050.2246781	+2.050.2246781	PROPN
eurjchem-1125	4	6	.	.	PUNCT
eurjchem-1125	4	7	e‐mail	e‐mail	PUNCT
eurjchem-1125	5	1	address	address	NOUN
eurjchem-1125	5	2	:	:	PUNCT
eurjchem-1125	5	3	dr_mostafa_chem@yahoo.com	dr_mostafa_chem@yahoo.com	X
eurjchem-1125	5	4	(	(	PUNCT
eurjchem-1125	5	5	m.a	m.a	PROPN
eurjchem-1125	5	6	.	.	PROPN
eurjchem-1125	5	7	gouda	gouda	NOUN
eurjchem-1125	5	8	)	)	PUNCT
eurjchem-1125	5	9	.	.	PUNCT
eurjchem-1125	6	1	article	article	NOUN
eurjchem-1125	6	2	information	information	PROPN
eurjchem-1125	6	3	abstract	abstract	ADJ
eurjchem-1125	6	4	doi	doi	NOUN
eurjchem-1125	6	5	:	:	PUNCT
eurjchem-1125	6	6	10.5155	10.5155	NUM
eurjchem-1125	6	7	/	/	SYM
eurjchem-1125	6	8	eurjchem.5.4.644‐651.1125	eurjchem.5.4.644‐651.1125	NUM
eurjchem-1125	6	9	received	receive	VERB
eurjchem-1125	6	10	:	:	PUNCT
eurjchem-1125	6	11	18	18	NUM
eurjchem-1125	6	12	july	july	PROPN
eurjchem-1125	6	13	2014	2014	NUM
eurjchem-1125	6	14	received	receive	VERB
eurjchem-1125	6	15	in	in	ADP
eurjchem-1125	6	16	revised	revise	VERB
eurjchem-1125	6	17	form	form	NOUN
eurjchem-1125	6	18	:	:	PUNCT
eurjchem-1125	6	19	05	05	NUM
eurjchem-1125	6	20	august	august	PROPN
eurjchem-1125	6	21	2014	2014	NUM
eurjchem-1125	6	22	accepted	accept	VERB
eurjchem-1125	6	23	:	:	PUNCT
eurjchem-1125	6	24	23	23	NUM
eurjchem-1125	6	25	august	august	PROPN
eurjchem-1125	6	26	2014	2014	NUM
eurjchem-1125	6	27	online	online	NOUN
eurjchem-1125	6	28	:	:	PUNCT
eurjchem-1125	6	29	31	31	NUM
eurjchem-1125	6	30	december	december	PROPN
eurjchem-1125	6	31	2014	2014	NUM
eurjchem-1125	6	32	keywords	keyword	VERB
eurjchem-1125	6	33	condensation	condensation	NOUN
eurjchem-1125	6	34	of	of	ADP
eurjchem-1125	6	35	cyanoacetamide	cyanoacetamide	ADJ
eurjchem-1125	6	36	3	3	NUM
eurjchem-1125	6	37	with	with	ADP
eurjchem-1125	6	38	cycloalkanones	cycloalkanone	NOUN
eurjchem-1125	6	39	and	and	CCONJ
eurjchem-1125	6	40	elemental	elemental	ADJ
eurjchem-1125	6	41	sulfur	sulfur	NOUN
eurjchem-1125	6	42	in	in	ADP
eurjchem-1125	6	43	the	the	DET
eurjchem-1125	6	44	presence	presence	NOUN
eurjchem-1125	6	45	of	of	ADP
eurjchem-1125	6	46	morpholine	morpholine	NOUN
eurjchem-1125	6	47	yielded	yield	VERB
eurjchem-1125	6	48	the	the	DET
eurjchem-1125	6	49	bisthiophenes	bisthiophene	NOUN
eurjchem-1125	6	50	4	4	NUM
eurjchem-1125	6	51	and	and	CCONJ
eurjchem-1125	6	52	5	5	NUM
eurjchem-1125	6	53	.	.	PUNCT
eurjchem-1125	7	1	also	also	ADV
eurjchem-1125	7	2	,	,	PUNCT
eurjchem-1125	7	3	its	its	PRON
eurjchem-1125	7	4	(	(	PUNCT
eurjchem-1125	7	5	3	3	NUM
eurjchem-1125	7	6	)	)	PUNCT
eurjchem-1125	7	7	condensation	condensation	NOUN
eurjchem-1125	7	8	with	with	ADP
eurjchem-1125	7	9	terphthalaldehyde	terphthalaldehyde	NOUN
eurjchem-1125	7	10	or	or	CCONJ
eurjchem-1125	7	11	coupling	couple	VERB
eurjchem-1125	7	12	with	with	ADP
eurjchem-1125	7	13	p‐phenylenedidiazonium	p‐phenylenedidiazonium	PUNCT
eurjchem-1125	7	14	chloride	chloride	NOUN
eurjchem-1125	7	15	afforded	afford	VERB
eurjchem-1125	7	16	compound	compound	NOUN
eurjchem-1125	7	17	13	13	NUM
eurjchem-1125	7	18	and	and	CCONJ
eurjchem-1125	7	19	14	14	NUM
eurjchem-1125	7	20	,	,	PUNCT
eurjchem-1125	7	21	respectively	respectively	ADV
eurjchem-1125	7	22	.	.	PUNCT
eurjchem-1125	8	1	furthermore	furthermore	ADV
eurjchem-1125	8	2	,	,	PUNCT
eurjchem-1125	8	3	cyanoacetylation	cyanoacetylation	NOUN
eurjchem-1125	8	4	of	of	ADP
eurjchem-1125	8	5	compound	compound	NOUN
eurjchem-1125	8	6	4	4	NUM
eurjchem-1125	8	7	or	or	CCONJ
eurjchem-1125	8	8	5	5	NUM
eurjchem-1125	8	9	afforded	afford	VERB
eurjchem-1125	8	10	the	the	DET
eurjchem-1125	8	11	cyanoacetamides	cyanoacetamide	NOUN
eurjchem-1125	8	12	6	6	NUM
eurjchem-1125	8	13	and	and	CCONJ
eurjchem-1125	8	14	7	7	NUM
eurjchem-1125	8	15	,	,	PUNCT
eurjchem-1125	8	16	respectively	respectively	ADV
eurjchem-1125	8	17	.	.	PUNCT
eurjchem-1125	9	1	knoevenagel	knoevenagel	NOUN
eurjchem-1125	9	2	condensation	condensation	NOUN
eurjchem-1125	9	3	of	of	ADP
eurjchem-1125	9	4	compound	compound	NOUN
eurjchem-1125	9	5	7	7	NUM
eurjchem-1125	9	6	with	with	ADP
eurjchem-1125	9	7	aromatic	aromatic	ADJ
eurjchem-1125	9	8	aldehyde	aldehyde	NOUN
eurjchem-1125	9	9	afforded	afford	VERB
eurjchem-1125	9	10	the	the	DET
eurjchem-1125	9	11	arylidenes	arylidene	NOUN
eurjchem-1125	9	12	10	10	NUM
eurjchem-1125	9	13	,	,	PUNCT
eurjchem-1125	9	14	11	11	NUM
eurjchem-1125	9	15	and	and	CCONJ
eurjchem-1125	9	16	coumarin	coumarin	NOUN
eurjchem-1125	9	17	12	12	NUM
eurjchem-1125	9	18	,	,	PUNCT
eurjchem-1125	9	19	respectively	respectively	ADV
eurjchem-1125	9	20	.	.	PUNCT
eurjchem-1125	10	1	treatment	treatment	NOUN
eurjchem-1125	10	2	of	of	ADP
eurjchem-1125	10	3	compound	compound	NOUN
eurjchem-1125	10	4	3	3	NUM
eurjchem-1125	10	5	with	with	ADP
eurjchem-1125	10	6	cs2	cs2	PROPN
eurjchem-1125	10	7	in	in	ADP
eurjchem-1125	10	8	dmf	dmf	PROPN
eurjchem-1125	10	9	/	/	SYM
eurjchem-1125	10	10	koh	koh	PROPN
eurjchem-1125	10	11	followed	follow	VERB
eurjchem-1125	10	12	by	by	ADP
eurjchem-1125	10	13	alkylation	alkylation	NOUN
eurjchem-1125	10	14	reaction	reaction	NOUN
eurjchem-1125	10	15	with	with	ADP
eurjchem-1125	10	16	ethyl	ethyl	PROPN
eurjchem-1125	10	17	bromoacetate	bromoacetate	NOUN
eurjchem-1125	10	18	afforded	afford	VERB
eurjchem-1125	10	19	the	the	DET
eurjchem-1125	10	20	triester	triester	NOUN
eurjchem-1125	10	21	derivative	derivative	ADJ
eurjchem-1125	10	22	16	16	NUM
eurjchem-1125	10	23	,	,	PUNCT
eurjchem-1125	10	24	which	which	PRON
eurjchem-1125	10	25	gave	give	VERB
eurjchem-1125	10	26	3‐aminothiophene	3‐aminothiophene	NUM
eurjchem-1125	10	27	17	17	NUM
eurjchem-1125	10	28	upon	upon	SCONJ
eurjchem-1125	10	29	heating	heating	NOUN
eurjchem-1125	10	30	in	in	ADP
eurjchem-1125	10	31	dmf	dmf	PROPN
eurjchem-1125	10	32	/	/	SYM
eurjchem-1125	10	33	tea	tea	NOUN
eurjchem-1125	10	34	.	.	PUNCT
eurjchem-1125	11	1	moreover	moreover	ADV
eurjchem-1125	11	2	,	,	PUNCT
eurjchem-1125	11	3	refluxing	refluxing	NOUN
eurjchem-1125	11	4	of	of	ADP
eurjchem-1125	11	5	compound	compound	NOUN
eurjchem-1125	11	6	23	23	NUM
eurjchem-1125	11	7	with	with	ADP
eurjchem-1125	11	8	α‐haloketones	α‐haloketone	NOUN
eurjchem-1125	11	9	afforded	afford	VERB
eurjchem-1125	11	10	3‐	3‐	NUM
eurjchem-1125	11	11	aminothiophenes	aminothiophene	NOUN
eurjchem-1125	11	12	24	24	NUM
eurjchem-1125	11	13	and	and	CCONJ
eurjchem-1125	11	14	25	25	NUM
eurjchem-1125	11	15	.	.	PUNCT
eurjchem-1125	11	16	identity	identity	NOUN
eurjchem-1125	11	17	of	of	ADP
eurjchem-1125	11	18	newly	newly	ADV
eurjchem-1125	11	19	synthesized	synthesize	VERB
eurjchem-1125	11	20	compounds	compound	NOUN
eurjchem-1125	11	21	was	be	AUX
eurjchem-1125	11	22	established	establish	VERB
eurjchem-1125	11	23	by	by	ADP
eurjchem-1125	11	24	the	the	DET
eurjchem-1125	11	25	spectral	spectral	ADJ
eurjchem-1125	11	26	data	datum	NOUN
eurjchem-1125	11	27	and	and	CCONJ
eurjchem-1125	11	28	novel	novel	ADJ
eurjchem-1125	11	29	compounds	compound	NOUN
eurjchem-1125	11	30	were	be	AUX
eurjchem-1125	11	31	evaluated	evaluate	VERB
eurjchem-1125	11	32	as	as	ADP
eurjchem-1125	11	33	antioxidant	antioxidant	ADJ
eurjchem-1125	11	34	agents	agent	NOUN
eurjchem-1125	11	35	.	.	PUNCT
eurjchem-1125	12	1	thiocarbamoyl	thiocarbamoyl	PROPN
eurjchem-1125	12	2	cyanoacetylation	cyanoacetylation	NOUN
eurjchem-1125	12	3	2‐aminothiophene	2‐aminothiophene	NUM
eurjchem-1125	12	4	antioxidant	antioxidant	ADJ
eurjchem-1125	12	5	evaluation	evaluation	NOUN
eurjchem-1125	12	6	3,5‐dimethyl‐1h‐pyrazole	3,5‐dimethyl‐1h‐pyrazole	NOUN
eurjchem-1125	12	7	3‐(ethoxycarbonyl)‐4,5,6,7‐tetrahydro‐1‐	3‐(ethoxycarbonyl)‐4,5,6,7‐tetrahydro‐1‐	NUM
eurjchem-1125	12	8	benzothiophen‐2‐amine	benzothiophen‐2‐amine	NOUN
eurjchem-1125	12	9	1	1	NUM
eurjchem-1125	12	10	.	.	PUNCT
eurjchem-1125	13	1	introduction	introduction	NOUN
eurjchem-1125	13	2	substituted	substitute	VERB
eurjchem-1125	13	3	2‐aminothiophenes	2‐aminothiophene	NOUN
eurjchem-1125	13	4	are	be	AUX
eurjchem-1125	13	5	important	important	ADJ
eurjchem-1125	13	6	interme‐	interme‐	NOUN
eurjchem-1125	13	7	diates	diate	NOUN
eurjchem-1125	13	8	in	in	ADP
eurjchem-1125	13	9	the	the	DET
eurjchem-1125	13	10	synthesis	synthesis	NOUN
eurjchem-1125	13	11	of	of	ADP
eurjchem-1125	13	12	a	a	DET
eurjchem-1125	13	13	variety	variety	NOUN
eurjchem-1125	13	14	of	of	ADP
eurjchem-1125	13	15	agrochemicals	agrochemical	NOUN
eurjchem-1125	13	16	,	,	PUNCT
eurjchem-1125	13	17	dyes	dye	NOUN
eurjchem-1125	13	18	and	and	CCONJ
eurjchem-1125	13	19	pharmacologically	pharmacologically	ADV
eurjchem-1125	13	20	active	active	ADJ
eurjchem-1125	13	21	compounds	compound	NOUN
eurjchem-1125	13	22	[	[	X
eurjchem-1125	13	23	1‐3	1‐3	NOUN
eurjchem-1125	13	24	]	]	PUNCT
eurjchem-1125	13	25	.	.	PUNCT
eurjchem-1125	14	1	the	the	DET
eurjchem-1125	14	2	most	most	ADV
eurjchem-1125	14	3	convergent	convergent	NOUN
eurjchem-1125	14	4	and	and	CCONJ
eurjchem-1125	14	5	well‐established	well‐establishe	VERB
eurjchem-1125	14	6	classical	classical	ADJ
eurjchem-1125	14	7	approach	approach	NOUN
eurjchem-1125	14	8	for	for	ADP
eurjchem-1125	14	9	the	the	DET
eurjchem-1125	14	10	preparation	preparation	NOUN
eurjchem-1125	14	11	of	of	ADP
eurjchem-1125	14	12	2‐aminothiophenes	2‐aminothiophene	NOUN
eurjchem-1125	14	13	is	be	AUX
eurjchem-1125	14	14	gewald	gewald	NOUN
eurjchem-1125	14	15	’s	’s	PART
eurjchem-1125	14	16	method	method	NOUN
eurjchem-1125	14	17	[	[	X
eurjchem-1125	14	18	4	4	NUM
eurjchem-1125	14	19	]	]	PUNCT
eurjchem-1125	14	20	,	,	PUNCT
eurjchem-1125	14	21	which	which	PRON
eurjchem-1125	14	22	involves	involve	VERB
eurjchem-1125	14	23	multicomponent	multicomponent	ADJ
eurjchem-1125	14	24	condensation	condensation	NOUN
eurjchem-1125	14	25	of	of	ADP
eurjchem-1125	14	26	a	a	DET
eurjchem-1125	14	27	ketone	ketone	NOUN
eurjchem-1125	14	28	with	with	ADP
eurjchem-1125	14	29	an	an	DET
eurjchem-1125	14	30	activated	activated	ADJ
eurjchem-1125	14	31	nitrile	nitrile	ADJ
eurjchem-1125	14	32	and	and	CCONJ
eurjchem-1125	14	33	elemental	elemental	ADJ
eurjchem-1125	14	34	sulfur	sulfur	NOUN
eurjchem-1125	14	35	in	in	ADP
eurjchem-1125	14	36	the	the	DET
eurjchem-1125	14	37	presence	presence	NOUN
eurjchem-1125	14	38	of	of	ADP
eurjchem-1125	14	39	morpholine	morpholine	NOUN
eurjchem-1125	14	40	as	as	ADP
eurjchem-1125	14	41	a	a	DET
eurjchem-1125	14	42	catalyst	catalyst	NOUN
eurjchem-1125	14	43	.	.	PUNCT
eurjchem-1125	15	1	3‐(3,5‐dimethyl‐1h‐pyrazol‐1‐yl)‐3‐	3‐(3,5‐dimethyl‐1h‐pyrazol‐1‐yl)‐3‐	NUM
eurjchem-1125	15	2	oxopropanenitrile	oxopropanenitrile	NOUN
eurjchem-1125	15	3	(	(	PUNCT
eurjchem-1125	15	4	2	2	NUM
eurjchem-1125	15	5	)	)	PUNCT
eurjchem-1125	15	6	is	be	AUX
eurjchem-1125	15	7	a	a	DET
eurjchem-1125	15	8	very	very	ADV
eurjchem-1125	15	9	handy	handy	ADJ
eurjchem-1125	15	10	and	and	CCONJ
eurjchem-1125	15	11	cheap	cheap	ADJ
eurjchem-1125	15	12	cyano	cyano	NOUN
eurjchem-1125	15	13	acetylation	acetylation	NOUN
eurjchem-1125	15	14	reagent	reagent	NOUN
eurjchem-1125	15	15	,	,	PUNCT
eurjchem-1125	15	16	which	which	PRON
eurjchem-1125	15	17	was	be	AUX
eurjchem-1125	15	18	first	first	ADV
eurjchem-1125	15	19	,	,	PUNCT
eurjchem-1125	15	20	synthesized	synthesize	VERB
eurjchem-1125	15	21	and	and	CCONJ
eurjchem-1125	15	22	introdu‐	introdu‐	NOUN
eurjchem-1125	15	23	ced	ce	VERB
eurjchem-1125	15	24	in	in	ADP
eurjchem-1125	15	25	common	common	ADJ
eurjchem-1125	15	26	practice	practice	NOUN
eurjchem-1125	15	27	in	in	ADP
eurjchem-1125	15	28	the	the	DET
eurjchem-1125	15	29	late	late	ADJ
eurjchem-1125	15	30	1950s	1950	NOUN
eurjchem-1125	15	31	by	by	ADP
eurjchem-1125	15	32	ried	rie	VERB
eurjchem-1125	15	33	and	and	CCONJ
eurjchem-1125	15	34	scheimer	scheimer	NOUN
eurjchem-1125	16	1	[	[	X
eurjchem-1125	16	2	5	5	NUM
eurjchem-1125	16	3	]	]	PUNCT
eurjchem-1125	16	4	.	.	PUNCT
eurjchem-1125	17	1	it	it	PRON
eurjchem-1125	17	2	was	be	AUX
eurjchem-1125	17	3	successfully	successfully	ADV
eurjchem-1125	17	4	applied	apply	VERB
eurjchem-1125	17	5	for	for	ADP
eurjchem-1125	17	6	the	the	DET
eurjchem-1125	17	7	synthesis	synthesis	NOUN
eurjchem-1125	17	8	of	of	ADP
eurjchem-1125	17	9	various	various	ADJ
eurjchem-1125	17	10	n‐	n‐	NOUN
eurjchem-1125	17	11	alkyl	alkyl	NOUN
eurjchem-1125	17	12	and	and	CCONJ
eurjchem-1125	17	13	n‐aryl	n‐aryl	X
eurjchem-1125	17	14	cyanoacetamides	cyanoacetamide	VERB
eurjchem-1125	17	15	[	[	X
eurjchem-1125	17	16	6	6	NUM
eurjchem-1125	17	17	]	]	PUNCT
eurjchem-1125	17	18	.	.	PUNCT
eurjchem-1125	18	1	recently	recently	ADV
eurjchem-1125	18	2	,	,	PUNCT
eurjchem-1125	18	3	gorobets	gorobet	NOUN
eurjchem-1125	18	4	et	et	PROPN
eurjchem-1125	18	5	al	al	PROPN
eurjchem-1125	18	6	.	.	PUNCT
eurjchem-1125	19	1	[	[	X
eurjchem-1125	19	2	7	7	NUM
eurjchem-1125	19	3	]	]	PUNCT
eurjchem-1125	19	4	,	,	PUNCT
eurjchem-1125	19	5	prepare	prepare	VERB
eurjchem-1125	19	6	a	a	DET
eurjchem-1125	19	7	series	series	NOUN
eurjchem-1125	19	8	from	from	ADP
eurjchem-1125	19	9	cyanoacetamides	cyanoacetamide	NOUN
eurjchem-1125	19	10	via	via	ADP
eurjchem-1125	19	11	refluxing	refluxing	NOUN
eurjchem-1125	19	12	of	of	ADP
eurjchem-1125	19	13	2	2	NUM
eurjchem-1125	19	14	with	with	ADP
eurjchem-1125	19	15	the	the	DET
eurjchem-1125	19	16	appropriate	appropriate	ADJ
eurjchem-1125	19	17	amines	amine	NOUN
eurjchem-1125	19	18	in	in	ADP
eurjchem-1125	19	19	toluene	toluene	NOUN
eurjchem-1125	19	20	.	.	PUNCT
eurjchem-1125	20	1	more	more	ADV
eurjchem-1125	20	2	recently	recently	ADV
eurjchem-1125	20	3	,	,	PUNCT
eurjchem-1125	20	4	we	we	PRON
eurjchem-1125	20	5	used	use	VERB
eurjchem-1125	20	6	compound	compound	NOUN
eurjchem-1125	20	7	2	2	NUM
eurjchem-1125	20	8	for	for	ADP
eurjchem-1125	20	9	preparation	preparation	NOUN
eurjchem-1125	20	10	of	of	ADP
eurjchem-1125	20	11	ethyl	ethyl	PROPN
eurjchem-1125	20	12	2‐(2‐cyano‐acetylamino)‐	2‐(2‐cyano‐acetylamino)‐	NUM
eurjchem-1125	20	13	4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxylate	4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxylate	NUM
eurjchem-1125	20	14	,	,	PUNCT
eurjchem-1125	20	15	3	3	NUM
eurjchem-1125	20	16	[	[	X
eurjchem-1125	20	17	8	8	NUM
eurjchem-1125	20	18	]	]	PUNCT
eurjchem-1125	20	19	.	.	PUNCT
eurjchem-1125	21	1	on	on	ADP
eurjchem-1125	21	2	the	the	DET
eurjchem-1125	21	3	other	other	ADJ
eurjchem-1125	21	4	hand	hand	NOUN
eurjchem-1125	21	5	,	,	PUNCT
eurjchem-1125	21	6	oxidative	oxidative	ADJ
eurjchem-1125	21	7	stress	stress	NOUN
eurjchem-1125	21	8	results	result	NOUN
eurjchem-1125	21	9	in	in	ADP
eurjchem-1125	21	10	oxidative	oxidative	ADJ
eurjchem-1125	21	11	alteration	alteration	NOUN
eurjchem-1125	21	12	of	of	ADP
eurjchem-1125	21	13	biological	biological	ADJ
eurjchem-1125	21	14	macromolecules	macromolecule	NOUN
eurjchem-1125	21	15	such	such	ADJ
eurjchem-1125	21	16	as	as	ADP
eurjchem-1125	21	17	lipids	lipid	NOUN
eurjchem-1125	21	18	,	,	PUNCT
eurjchem-1125	21	19	proteins	protein	NOUN
eurjchem-1125	21	20	and	and	CCONJ
eurjchem-1125	21	21	nucleic	nucleic	ADJ
eurjchem-1125	21	22	acids	acid	NOUN
eurjchem-1125	21	23	.	.	PUNCT
eurjchem-1125	22	1	it	it	PRON
eurjchem-1125	22	2	is	be	AUX
eurjchem-1125	22	3	considered	consider	VERB
eurjchem-1125	22	4	to	to	PART
eurjchem-1125	22	5	play	play	VERB
eurjchem-1125	22	6	a	a	DET
eurjchem-1125	22	7	pivotal	pivotal	ADJ
eurjchem-1125	22	8	role	role	NOUN
eurjchem-1125	22	9	in	in	ADP
eurjchem-1125	22	10	the	the	DET
eurjchem-1125	22	11	pathogenesis	pathogenesis	NOUN
eurjchem-1125	22	12	of	of	ADP
eurjchem-1125	22	13	aging	age	VERB
eurjchem-1125	22	14	and	and	CCONJ
eurjchem-1125	22	15	degenerative	degenerative	ADJ
eurjchem-1125	22	16	diseases	disease	NOUN
eurjchem-1125	22	17	[	[	X
eurjchem-1125	22	18	9‐11	9‐11	X
eurjchem-1125	22	19	]	]	PUNCT
eurjchem-1125	22	20	.	.	PUNCT
eurjchem-1125	23	1	in	in	ADP
eurjchem-1125	23	2	order	order	NOUN
eurjchem-1125	23	3	to	to	PART
eurjchem-1125	23	4	cope	cope	VERB
eurjchem-1125	23	5	with	with	ADP
eurjchem-1125	23	6	an	an	DET
eurjchem-1125	23	7	excess	excess	NOUN
eurjchem-1125	23	8	of	of	ADP
eurjchem-1125	23	9	free	free	ADJ
eurjchem-1125	23	10	radicals	radical	NOUN
eurjchem-1125	23	11	produced	produce	VERB
eurjchem-1125	23	12	upon	upon	SCONJ
eurjchem-1125	23	13	oxidative	oxidative	ADJ
eurjchem-1125	23	14	stress	stress	NOUN
eurjchem-1125	23	15	,	,	PUNCT
eurjchem-1125	23	16	human	human	ADJ
eurjchem-1125	23	17	bodies	body	NOUN
eurjchem-1125	23	18	have	have	AUX
eurjchem-1125	23	19	developed	develop	VERB
eurjchem-1125	23	20	sophisticated	sophisticated	ADJ
eurjchem-1125	23	21	mechanisms	mechanism	NOUN
eurjchem-1125	23	22	for	for	ADP
eurjchem-1125	23	23	maintaining	maintain	VERB
eurjchem-1125	23	24	redox	redox	NOUN
eurjchem-1125	23	25	homeostasis	homeostasis	NOUN
eurjchem-1125	23	26	.	.	PUNCT
eurjchem-1125	24	1	these	these	DET
eurjchem-1125	24	2	protective	protective	ADJ
eurjchem-1125	24	3	mechanisms	mechanism	NOUN
eurjchem-1125	24	4	include	include	VERB
eurjchem-1125	24	5	scavenging	scavenge	VERB
eurjchem-1125	24	6	or	or	CCONJ
eurjchem-1125	24	7	detoxification	detoxification	NOUN
eurjchem-1125	24	8	of	of	ADP
eurjchem-1125	24	9	reactive	reactive	ADJ
eurjchem-1125	24	10	oxygen	oxygen	NOUN
eurjchem-1125	24	11	species	specie	NOUN
eurjchem-1125	24	12	(	(	PUNCT
eurjchem-1125	24	13	ros	ros	PROPN
eurjchem-1125	24	14	)	)	PUNCT
eurjchem-1125	24	15	,	,	PUNCT
eurjchem-1125	24	16	blocking	block	VERB
eurjchem-1125	24	17	ros	ros	PROPN
eurjchem-1125	24	18	production	production	NOUN
eurjchem-1125	24	19	,	,	PUNCT
eurjchem-1125	24	20	sequestration	sequestration	NOUN
eurjchem-1125	24	21	of	of	ADP
eurjchem-1125	24	22	transition	transition	NOUN
eurjchem-1125	24	23	metals	metal	NOUN
eurjchem-1125	24	24	,	,	PUNCT
eurjchem-1125	24	25	as	as	ADV
eurjchem-1125	24	26	well	well	ADV
eurjchem-1125	24	27	as	as	ADP
eurjchem-1125	24	28	enzymatic	enzymatic	ADJ
eurjchem-1125	24	29	and	and	CCONJ
eurjchem-1125	24	30	nonenzymatic	nonenzymatic	ADJ
eurjchem-1125	24	31	antioxidant	antioxidant	NOUN
eurjchem-1125	24	32	defenses	defense	NOUN
eurjchem-1125	24	33	produced	produce	VERB
eurjchem-1125	24	34	in	in	ADP
eurjchem-1125	24	35	the	the	DET
eurjchem-1125	24	36	body	body	NOUN
eurjchem-1125	24	37	,	,	PUNCT
eurjchem-1125	24	38	that	that	ADV
eurjchem-1125	24	39	is	is	ADV
eurjchem-1125	24	40	,	,	PUNCT
eurjchem-1125	24	41	endogenous	endogenous	ADJ
eurjchem-1125	24	42	[	[	X
eurjchem-1125	24	43	12,13	12,13	NUM
eurjchem-1125	24	44	]	]	PUNCT
eurjchem-1125	24	45	and	and	CCONJ
eurjchem-1125	24	46	others	other	NOUN
eurjchem-1125	24	47	supplied	supply	VERB
eurjchem-1125	24	48	with	with	ADP
eurjchem-1125	24	49	the	the	DET
eurjchem-1125	24	50	diet	diet	NOUN
eurjchem-1125	24	51	,	,	PUNCT
eurjchem-1125	24	52	namely	namely	ADV
eurjchem-1125	24	53	,	,	PUNCT
eurjchem-1125	24	54	exogenous	exogenous	ADJ
eurjchem-1125	24	55	ones	one	NOUN
eurjchem-1125	24	56	.	.	PUNCT
eurjchem-1125	25	1	among	among	ADP
eurjchem-1125	25	2	them	they	PRON
eurjchem-1125	25	3	,	,	PUNCT
eurjchem-1125	25	4	dietary	dietary	ADJ
eurjchem-1125	25	5	polyphenols	polyphenol	NOUN
eurjchem-1125	25	6	have	have	AUX
eurjchem-1125	25	7	been	be	AUX
eurjchem-1125	25	8	widely	widely	ADV
eurjchem-1125	25	9	studied	study	VERB
eurjchem-1125	25	10	for	for	ADP
eurjchem-1125	25	11	their	their	PRON
eurjchem-1125	25	12	strong	strong	ADJ
eurjchem-1125	25	13	antioxidant	antioxidant	ADJ
eurjchem-1125	25	14	capacities	capacity	NOUN
eurjchem-1125	25	15	and	and	CCONJ
eurjchem-1125	25	16	other	other	ADJ
eurjchem-1125	25	17	properties	property	NOUN
eurjchem-1125	25	18	by	by	ADP
eurjchem-1125	25	19	which	which	PRON
eurjchem-1125	25	20	cell	cell	NOUN
eurjchem-1125	25	21	functions	function	NOUN
eurjchem-1125	25	22	are	be	AUX
eurjchem-1125	25	23	regulated	regulate	VERB
eurjchem-1125	25	24	[	[	PUNCT
eurjchem-1125	25	25	14	14	NUM
eurjchem-1125	25	26	,	,	PUNCT
eurjchem-1125	25	27	15	15	NUM
eurjchem-1125	25	28	]	]	PUNCT
eurjchem-1125	25	29	.	.	PUNCT
eurjchem-1125	26	1	recently	recently	ADV
eurjchem-1125	26	2	,	,	PUNCT
eurjchem-1125	26	3	thiophenecarbohydrazide	thiophenecarbohydrazide	ADJ
eurjchem-1125	26	4	,	,	PUNCT
eurjchem-1125	26	5	thienopyrazole	thienopyrazole	NOUN
eurjchem-1125	26	6	and	and	CCONJ
eurjchem-1125	26	7	thienopyrimidine	thienopyrimidine	NOUN
eurjchem-1125	26	8	derivatives	derivative	NOUN
eurjchem-1125	26	9	showed	show	VERB
eurjchem-1125	26	10	interesting	interesting	ADJ
eurjchem-1125	26	11	biological	biological	ADJ
eurjchem-1125	26	12	properties	property	NOUN
eurjchem-1125	26	13	including	include	VERB
eurjchem-1125	26	14	antioxidant	antioxidant	ADJ
eurjchem-1125	26	15	and	and	CCONJ
eurjchem-1125	26	16	antitumor	antitumor	NOUN
eurjchem-1125	26	17	activities	activity	NOUN
eurjchem-1125	26	18	[	[	X
eurjchem-1125	26	19	16	16	NUM
eurjchem-1125	26	20	]	]	PUNCT
eurjchem-1125	26	21	.	.	PUNCT
eurjchem-1125	27	1	in	in	ADP
eurjchem-1125	27	2	view	view	NOUN
eurjchem-1125	27	3	of	of	ADP
eurjchem-1125	27	4	the	the	DET
eurjchem-1125	27	5	above	above	ADJ
eurjchem-1125	27	6	result	result	NOUN
eurjchem-1125	27	7	we	we	PRON
eurjchem-1125	27	8	use	use	VERB
eurjchem-1125	27	9	herein	herein	NOUN
eurjchem-1125	27	10	3	3	NUM
eurjchem-1125	27	11	as	as	ADP
eurjchem-1125	27	12	a	a	DET
eurjchem-1125	27	13	building	building	NOUN
eurjchem-1125	27	14	block	block	NOUN
eurjchem-1125	27	15	for	for	ADP
eurjchem-1125	27	16	the	the	DET
eurjchem-1125	27	17	construction	construction	NOUN
eurjchem-1125	27	18	of	of	ADP
eurjchem-1125	27	19	poly‐thiophene	poly‐thiophene	NOUN
eurjchem-1125	27	20	ring	ring	NOUN
eurjchem-1125	27	21	systems	system	NOUN
eurjchem-1125	27	22	in	in	ADP
eurjchem-1125	27	23	order	order	NOUN
eurjchem-1125	27	24	to	to	PART
eurjchem-1125	27	25	evaluate	evaluate	VERB
eurjchem-1125	27	26	their	their	PRON
eurjchem-1125	27	27	antioxidant	antioxidant	ADJ
eurjchem-1125	27	28	activity	activity	NOUN
eurjchem-1125	27	29	.	.	PUNCT
eurjchem-1125	28	1	2	2	X
eurjchem-1125	28	2	.	.	X
eurjchem-1125	28	3	experimental	experimental	ADJ
eurjchem-1125	28	4	2.1	2.1	NUM
eurjchem-1125	28	5	.	.	PUNCT
eurjchem-1125	29	1	instrumentations	instrumentation	NOUN
eurjchem-1125	29	2	all	all	DET
eurjchem-1125	29	3	melting	melt	VERB
eurjchem-1125	29	4	points	point	NOUN
eurjchem-1125	29	5	are	be	AUX
eurjchem-1125	29	6	determined	determine	VERB
eurjchem-1125	29	7	on	on	ADP
eurjchem-1125	29	8	gallenkamp	gallenkamp	ADJ
eurjchem-1125	29	9	electric	electric	ADJ
eurjchem-1125	29	10	melting	melting	NOUN
eurjchem-1125	29	11	point	point	NOUN
eurjchem-1125	29	12	apparatus	apparatus	NOUN
eurjchem-1125	29	13	(	(	PUNCT
eurjchem-1125	29	14	uncorrected	uncorrected	ADJ
eurjchem-1125	29	15	)	)	PUNCT
eurjchem-1125	29	16	.	.	PUNCT
eurjchem-1125	30	1	gouda	gouda	NOUN
eurjchem-1125	30	2	and	and	CCONJ
eurjchem-1125	30	3	el‐bialy	el‐bialy	PROPN
eurjchem-1125	30	4	/	/	SYM
eurjchem-1125	30	5	european	european	PROPN
eurjchem-1125	30	6	journal	journal	PROPN
eurjchem-1125	30	7	of	of	ADP
eurjchem-1125	30	8	chemistry	chemistry	NOUN
eurjchem-1125	30	9	5	5	NUM
eurjchem-1125	30	10	(	(	PUNCT
eurjchem-1125	30	11	4	4	NUM
eurjchem-1125	30	12	)	)	PUNCT
eurjchem-1125	30	13	(	(	PUNCT
eurjchem-1125	30	14	2014	2014	NUM
eurjchem-1125	30	15	)	)	PUNCT
eurjchem-1125	31	1	644‐651	644‐651	NUM
eurjchem-1125	31	2	645	645	NUM
eurjchem-1125	31	3	scheme	scheme	NOUN
eurjchem-1125	31	4	1	1	NUM
eurjchem-1125	31	5	thin	thin	ADJ
eurjchem-1125	31	6	layer	layer	NOUN
eurjchem-1125	31	7	chroma‐tography	chroma‐tography	NOUN
eurjchem-1125	31	8	(	(	PUNCT
eurjchem-1125	31	9	tlc	tlc	NOUN
eurjchem-1125	31	10	)	)	PUNCT
eurjchem-1125	31	11	analysis	analysis	NOUN
eurjchem-1125	31	12	was	be	AUX
eurjchem-1125	31	13	carried	carry	VERB
eurjchem-1125	31	14	out	out	ADP
eurjchem-1125	31	15	on	on	ADP
eurjchem-1125	31	16	silica	silica	NOUN
eurjchem-1125	31	17	gel	gel	NOUN
eurjchem-1125	31	18	60f254	60f254	NOUN
eurjchem-1125	31	19	precoated	precoate	VERB
eurjchem-1125	31	20	aluminum	aluminum	NOUN
eurjchem-1125	31	21	sheets	sheet	NOUN
eurjchem-1125	31	22	.	.	PUNCT
eurjchem-1125	32	1	the	the	DET
eurjchem-1125	32	2	ir	ir	PROPN
eurjchem-1125	32	3	spectra	spectra	PROPN
eurjchem-1125	32	4	were	be	AUX
eurjchem-1125	32	5	recorded	record	VERB
eurjchem-1125	32	6	(	(	PUNCT
eurjchem-1125	32	7	kbr	kbr	PROPN
eurjchem-1125	32	8	)	)	PUNCT
eurjchem-1125	32	9	on	on	ADP
eurjchem-1125	32	10	a	a	DET
eurjchem-1125	32	11	mattson	mattson	NOUN
eurjchem-1125	32	12	5000	5000	NUM
eurjchem-1125	32	13	ftir	ftir	PROPN
eurjchem-1125	32	14	spectrophoto‐	spectrophoto‐	PROPN
eurjchem-1125	32	15	meter	meter	NOUN
eurjchem-1125	32	16	at	at	ADP
eurjchem-1125	32	17	the	the	DET
eurjchem-1125	32	18	microanalytical	microanalytical	ADJ
eurjchem-1125	32	19	unit	unit	NOUN
eurjchem-1125	32	20	,	,	PUNCT
eurjchem-1125	32	21	faculty	faculty	NOUN
eurjchem-1125	32	22	of	of	ADP
eurjchem-1125	32	23	science	science	NOUN
eurjchem-1125	32	24	,	,	PUNCT
eurjchem-1125	32	25	mansoura	mansoura	PROPN
eurjchem-1125	32	26	university	university	PROPN
eurjchem-1125	32	27	1h/13c	1h/13c	PROPN
eurjchem-1125	32	28	nmr	nmr	PROPN
eurjchem-1125	32	29	spectra	spectra	NOUN
eurjchem-1125	32	30	were	be	AUX
eurjchem-1125	32	31	recorded	record	VERB
eurjchem-1125	32	32	at	at	ADP
eurjchem-1125	32	33	400	400	NUM
eurjchem-1125	32	34	and	and	CCONJ
eurjchem-1125	32	35	100	100	NUM
eurjchem-1125	32	36	mhz	mhz	NOUN
eurjchem-1125	32	37	,	,	PUNCT
eurjchem-1125	32	38	respectively	respectively	ADV
eurjchem-1125	32	39	,	,	PUNCT
eurjchem-1125	32	40	on	on	ADP
eurjchem-1125	32	41	a	a	DET
eurjchem-1125	32	42	bruker	bruker	NOUN
eurjchem-1125	32	43	400	400	NUM
eurjchem-1125	32	44	nmr	nmr	NOUN
eurjchem-1125	32	45	spectrometer	spectrometer	NOUN
eurjchem-1125	32	46	in	in	ADP
eurjchem-1125	32	47	the	the	DET
eurjchem-1125	32	48	indicated	indicate	VERB
eurjchem-1125	32	49	solvents	solvent	NOUN
eurjchem-1125	32	50	using	use	VERB
eurjchem-1125	32	51	tms	tms	PROPN
eurjchem-1125	32	52	as	as	ADP
eurjchem-1125	32	53	an	an	DET
eurjchem-1125	32	54	internal	internal	ADJ
eurjchem-1125	32	55	reference	reference	NOUN
eurjchem-1125	32	56	,	,	PUNCT
eurjchem-1125	32	57	at	at	ADP
eurjchem-1125	32	58	the	the	DET
eurjchem-1125	32	59	georgia	georgia	PROPN
eurjchem-1125	32	60	state	state	PROPN
eurjchem-1125	32	61	university	university	PROPN
eurjchem-1125	32	62	,	,	PUNCT
eurjchem-1125	32	63	atlanta	atlanta	PROPN
eurjchem-1125	32	64	,	,	PUNCT
eurjchem-1125	32	65	georgia	georgia	PROPN
eurjchem-1125	32	66	,	,	PUNCT
eurjchem-1125	32	67	usa	usa	PROPN
eurjchem-1125	32	68	.	.	PUNCT
eurjchem-1125	33	1	the	the	DET
eurjchem-1125	33	2	mass	mass	ADJ
eurjchem-1125	33	3	spectra	spectra	NOUN
eurjchem-1125	33	4	(	(	PUNCT
eurjchem-1125	33	5	ei	ei	NOUN
eurjchem-1125	33	6	)	)	PUNCT
eurjchem-1125	33	7	were	be	AUX
eurjchem-1125	33	8	recorded	record	VERB
eurjchem-1125	33	9	on	on	ADP
eurjchem-1125	33	10	kratos	kratos	PROPN
eurjchem-1125	33	11	ms	ms	PROPN
eurjchem-1125	33	12	equipment	equipment	NOUN
eurjchem-1125	33	13	at	at	ADP
eurjchem-1125	33	14	the	the	DET
eurjchem-1125	33	15	microanalytical	microanalytical	ADJ
eurjchem-1125	33	16	center	center	NOUN
eurjchem-1125	33	17	,	,	PUNCT
eurjchem-1125	33	18	cairo	cairo	PROPN
eurjchem-1125	33	19	university	university	PROPN
eurjchem-1125	33	20	,	,	PUNCT
eurjchem-1125	33	21	egypt	egypt	PROPN
eurjchem-1125	33	22	.	.	PUNCT
eurjchem-1125	34	1	elemental	elemental	ADJ
eurjchem-1125	34	2	analyses	analysis	NOUN
eurjchem-1125	34	3	(	(	PUNCT
eurjchem-1125	34	4	c	c	X
eurjchem-1125	34	5	,	,	PUNCT
eurjchem-1125	34	6	h	h	NOUN
eurjchem-1125	34	7	and	and	CCONJ
eurjchem-1125	34	8	n	n	CCONJ
eurjchem-1125	34	9	)	)	PUNCT
eurjchem-1125	34	10	were	be	AUX
eurjchem-1125	34	11	carried	carry	VERB
eurjchem-1125	34	12	out	out	ADP
eurjchem-1125	34	13	at	at	ADP
eurjchem-1125	34	14	the	the	DET
eurjchem-1125	34	15	microanalytical	microanalytical	ADJ
eurjchem-1125	34	16	center	center	NOUN
eurjchem-1125	34	17	of	of	ADP
eurjchem-1125	34	18	cairo	cairo	PROPN
eurjchem-1125	34	19	university	university	PROPN
eurjchem-1125	34	20	,	,	PUNCT
eurjchem-1125	34	21	egypt	egypt	PROPN
eurjchem-1125	34	22	.	.	PUNCT
eurjchem-1125	35	1	biological	biological	ADJ
eurjchem-1125	35	2	activities	activity	NOUN
eurjchem-1125	35	3	were	be	AUX
eurjchem-1125	35	4	carried	carry	VERB
eurjchem-1125	35	5	out	out	ADP
eurjchem-1125	35	6	at	at	ADP
eurjchem-1125	35	7	pharmacognosy	pharmacognosy	PROPN
eurjchem-1125	35	8	department	department	NOUN
eurjchem-1125	35	9	,	,	PUNCT
eurjchem-1125	35	10	faculty	faculty	NOUN
eurjchem-1125	35	11	of	of	ADP
eurjchem-1125	35	12	pharmacy	pharmacy	NOUN
eurjchem-1125	35	13	,	,	PUNCT
eurjchem-1125	35	14	mansoura	mansoura	PROPN
eurjchem-1125	35	15	university	university	NOUN
eurjchem-1125	35	16	,	,	PUNCT
eurjchem-1125	35	17	mansoura	mansoura	PROPN
eurjchem-1125	35	18	,	,	PUNCT
eurjchem-1125	35	19	egypt	egypt	PROPN
eurjchem-1125	35	20	.	.	PUNCT
eurjchem-1125	36	1	ethyl	ethyl	PROPN
eurjchem-1125	36	2	2‐	2‐	NUM
eurjchem-1125	37	1	amino‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxy	amino‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxy	DET
eurjchem-1125	37	2	late	late	ADV
eurjchem-1125	37	3	(	(	PUNCT
eurjchem-1125	37	4	1	1	X
eurjchem-1125	37	5	)	)	PUNCT
eurjchem-1125	37	6	[	[	X
eurjchem-1125	37	7	17	17	NUM
eurjchem-1125	37	8	]	]	PUNCT
eurjchem-1125	37	9	,	,	PUNCT
eurjchem-1125	37	10	ethyl	ethyl	PROPN
eurjchem-1125	37	11	2‐[(cyanoacetyl)amino]‐4,5,6,7‐tetrahydro‐1‐benzo	2‐[(cyanoacetyl)amino]‐4,5,6,7‐tetrahydro‐1‐benzo	PROPN
eurjchem-1125	37	12	thiophene‐3‐carboxylate	thiophene‐3‐carboxylate	NUM
eurjchem-1125	37	13	(	(	PUNCT
eurjchem-1125	37	14	3	3	NUM
eurjchem-1125	37	15	)	)	PUNCT
eurjchem-1125	37	16	[	[	X
eurjchem-1125	37	17	8	8	NUM
eurjchem-1125	37	18	]	]	PUNCT
eurjchem-1125	37	19	and	and	CCONJ
eurjchem-1125	37	20	(	(	PUNCT
eurjchem-1125	37	21	z)‐ethyl	z)‐ethyl	PROPN
eurjchem-1125	37	22	2‐(2‐cyano‐3‐	2‐(2‐cyano‐3‐	NUM
eurjchem-1125	37	23	mercapto‐3‐(phenylamino)acrylamido)‐4	mercapto‐3‐(phenylamino)acrylamido)‐4	PROPN
eurjchem-1125	37	24	,	,	PUNCT
eurjchem-1125	37	25	5	5	NUM
eurjchem-1125	37	26	,	,	PUNCT
eurjchem-1125	37	27	6	6	NUM
eurjchem-1125	37	28	,	,	PUNCT
eurjchem-1125	37	29	7‐tetrahydro	7‐tetrahydro	NUM
eurjchem-1125	37	30	benzo[b]thiophene‐3‐carboxylate	benzo[b]thiophene‐3‐carboxylate	NOUN
eurjchem-1125	37	31	(	(	PUNCT
eurjchem-1125	37	32	23	23	NUM
eurjchem-1125	37	33	)	)	PUNCT
eurjchem-1125	38	1	[	[	X
eurjchem-1125	38	2	8	8	NUM
eurjchem-1125	38	3	]	]	PUNCT
eurjchem-1125	38	4	were	be	AUX
eurjchem-1125	38	5	reported	report	VERB
eurjchem-1125	38	6	in	in	ADP
eurjchem-1125	38	7	the	the	DET
eurjchem-1125	38	8	literature	literature	NOUN
eurjchem-1125	38	9	2.2	2.2	NUM
eurjchem-1125	38	10	.	.	PUNCT
eurjchem-1125	39	1	synthesis	synthesis	NOUN
eurjchem-1125	39	2	2.2.1	2.2.1	NUM
eurjchem-1125	39	3	.	.	PUNCT
eurjchem-1125	40	1	reaction	reaction	NOUN
eurjchem-1125	40	2	of	of	ADP
eurjchem-1125	40	3	ethyl	ethyl	PROPN
eurjchem-1125	40	4	2‐[(cyanoacetyl	2‐[(cyanoacetyl	NUM
eurjchem-1125	40	5	)	)	PUNCT
eurjchem-1125	40	6	amino]‐4,5,6,7‐tetra	amino]‐4,5,6,7‐tetra	PROPN
eurjchem-1125	40	7	hydro‐1‐benzothiophene‐3‐carboxylate	hydro‐1‐benzothiophene‐3‐carboxylate	NOUN
eurjchem-1125	40	8	(	(	PUNCT
eurjchem-1125	40	9	3	3	NUM
eurjchem-1125	40	10	)	)	PUNCT
eurjchem-1125	40	11	with	with	ADP
eurjchem-1125	40	12	cyclic	cyclic	ADJ
eurjchem-1125	40	13	ketones	ketone	NOUN
eurjchem-1125	40	14	and	and	CCONJ
eurjchem-1125	40	15	elemental	elemental	ADJ
eurjchem-1125	40	16	sulfur	sulfur	NOUN
eurjchem-1125	40	17	general	general	ADJ
eurjchem-1125	40	18	procedure	procedure	NOUN
eurjchem-1125	40	19	:	:	PUNCT
eurjchem-1125	40	20	morpholine	morpholine	NOUN
eurjchem-1125	40	21	(	(	PUNCT
eurjchem-1125	40	22	0.33	0.33	NUM
eurjchem-1125	40	23	ml	ml	NOUN
eurjchem-1125	40	24	,	,	PUNCT
eurjchem-1125	40	25	3.9	3.9	NUM
eurjchem-1125	40	26	mmol	mmol	NOUN
eurjchem-1125	40	27	)	)	PUNCT
eurjchem-1125	40	28	,	,	PUNCT
eurjchem-1125	40	29	elemental	elemental	ADJ
eurjchem-1125	40	30	sulfur	sulfur	NOUN
eurjchem-1125	40	31	(	(	PUNCT
eurjchem-1125	40	32	0.141	0.141	NUM
eurjchem-1125	40	33	g	g	NOUN
eurjchem-1125	40	34	,	,	PUNCT
eurjchem-1125	40	35	4.4	4.4	NUM
eurjchem-1125	40	36	mmol	mmol	NOUN
eurjchem-1125	40	37	)	)	PUNCT
eurjchem-1125	40	38	and	and	CCONJ
eurjchem-1125	40	39	cyclopentanone	cyclopentanone	NOUN
eurjchem-1125	40	40	(	(	PUNCT
eurjchem-1125	40	41	0.34	0.34	NUM
eurjchem-1125	40	42	g	g	NOUN
eurjchem-1125	40	43	,	,	PUNCT
eurjchem-1125	40	44	4	4	NUM
eurjchem-1125	40	45	mmol	mmol	NOUN
eurjchem-1125	40	46	)	)	PUNCT
eurjchem-1125	40	47	or	or	CCONJ
eurjchem-1125	40	48	cyclohexanone	cyclohexanone	NOUN
eurjchem-1125	40	49	(	(	PUNCT
eurjchem-1125	40	50	0.39	0.39	NUM
eurjchem-1125	40	51	g	g	NOUN
eurjchem-1125	40	52	,	,	PUNCT
eurjchem-1125	40	53	4	4	NUM
eurjchem-1125	40	54	mmol	mmol	NOUN
eurjchem-1125	40	55	)	)	PUNCT
eurjchem-1125	40	56	were	be	AUX
eurjchem-1125	40	57	added	add	VERB
eurjchem-1125	40	58	to	to	ADP
eurjchem-1125	40	59	a	a	DET
eurjchem-1125	40	60	solution	solution	NOUN
eurjchem-1125	40	61	of	of	ADP
eurjchem-1125	40	62	compound	compound	NOUN
eurjchem-1125	40	63	3	3	NUM
eurjchem-1125	40	64	(	(	PUNCT
eurjchem-1125	40	65	1.17	1.17	NUM
eurjchem-1125	40	66	g	g	NOUN
eurjchem-1125	40	67	,	,	PUNCT
eurjchem-1125	40	68	4	4	NUM
eurjchem-1125	40	69	mmol	mmol	NOUN
eurjchem-1125	40	70	)	)	PUNCT
eurjchem-1125	40	71	in	in	ADP
eurjchem-1125	40	72	ethanol	ethanol	NOUN
eurjchem-1125	40	73	(	(	PUNCT
eurjchem-1125	40	74	20	20	NUM
eurjchem-1125	40	75	ml	ml	NOUN
eurjchem-1125	40	76	)	)	PUNCT
eurjchem-1125	40	77	.	.	PUNCT
eurjchem-1125	41	1	the	the	DET
eurjchem-1125	41	2	reaction	reaction	NOUN
eurjchem-1125	41	3	mixture	mixture	NOUN
eurjchem-1125	41	4	was	be	AUX
eurjchem-1125	41	5	refluxed	refluxe	VERB
eurjchem-1125	41	6	at	at	ADP
eurjchem-1125	41	7	60‐80	60‐80	NOUN
eurjchem-1125	41	8	°	°	ADP
eurjchem-1125	41	9	c	c	PROPN
eurjchem-1125	41	10	for	for	ADP
eurjchem-1125	41	11	6	6	NUM
eurjchem-1125	41	12	h	h	NOUN
eurjchem-1125	41	13	and	and	CCONJ
eurjchem-1125	41	14	left	leave	VERB
eurjchem-1125	41	15	to	to	PART
eurjchem-1125	41	16	stand	stand	VERB
eurjchem-1125	41	17	at	at	ADP
eurjchem-1125	41	18	room	room	NOUN
eurjchem-1125	41	19	temperature	temperature	NOUN
eurjchem-1125	41	20	.	.	PUNCT
eurjchem-1125	42	1	the	the	DET
eurjchem-1125	42	2	separated	separate	VERB
eurjchem-1125	42	3	crystalline	crystalline	NOUN
eurjchem-1125	42	4	product	product	NOUN
eurjchem-1125	42	5	was	be	AUX
eurjchem-1125	42	6	filtered	filter	VERB
eurjchem-1125	42	7	,	,	PUNCT
eurjchem-1125	42	8	dried	dry	VERB
eurjchem-1125	42	9	and	and	CCONJ
eurjchem-1125	42	10	recrystallized	recrystallize	VERB
eurjchem-1125	42	11	from	from	ADP
eurjchem-1125	42	12	ethanol	ethanol	NOUN
eurjchem-1125	42	13	:	:	PUNCT
eurjchem-1125	42	14	benzene	benzene	NOUN
eurjchem-1125	42	15	mixture	mixture	NOUN
eurjchem-1125	42	16	(	(	PUNCT
eurjchem-1125	42	17	3:2	3:2	NUM
eurjchem-1125	42	18	,	,	PUNCT
eurjchem-1125	42	19	v	v	NOUN
eurjchem-1125	42	20	:	:	SYM
eurjchem-1125	42	21	v	v	NOUN
eurjchem-1125	42	22	)	)	PUNCT
eurjchem-1125	42	23	to	to	PART
eurjchem-1125	42	24	give	give	VERB
eurjchem-1125	42	25	compounds	compound	NOUN
eurjchem-1125	42	26	4	4	NUM
eurjchem-1125	42	27	and	and	CCONJ
eurjchem-1125	42	28	5	5	NUM
eurjchem-1125	42	29	,	,	PUNCT
eurjchem-1125	42	30	respectively	respectively	ADV
eurjchem-1125	42	31	(	(	PUNCT
eurjchem-1125	42	32	scheme	scheme	NOUN
eurjchem-1125	42	33	1	1	NUM
eurjchem-1125	42	34	)	)	PUNCT
eurjchem-1125	42	35	.	.	PUNCT
eurjchem-1125	43	1	ethyl	ethyl	PROPN
eurjchem-1125	43	2	2‐{[(2‐amino‐5,6‐dihydro‐4h‐cyclopenta[b]thien‐3‐yl	2‐{[(2‐amino‐5,6‐dihydro‐4h‐cyclopenta[b]thien‐3‐yl	PROPN
eurjchem-1125	43	3	)	)	PUNCT
eurjchem-1125	43	4	carbonyl]amino}‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxy	carbonyl]amino}‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxy	ADJ
eurjchem-1125	43	5	late	late	ADV
eurjchem-1125	43	6	(	(	PUNCT
eurjchem-1125	43	7	4	4	NUM
eurjchem-1125	43	8	):	):	PUNCT
eurjchem-1125	43	9	color	color	NOUN
eurjchem-1125	43	10	:	:	PUNCT
eurjchem-1125	43	11	white	white	ADJ
eurjchem-1125	43	12	powder	powder	NOUN
eurjchem-1125	43	13	.	.	PUNCT
eurjchem-1125	44	1	yield	yield	NOUN
eurjchem-1125	44	2	:	:	PUNCT
eurjchem-1125	44	3	1.39	1.39	NUM
eurjchem-1125	44	4	g	g	NOUN
eurjchem-1125	44	5	,	,	PUNCT
eurjchem-1125	44	6	89	89	NUM
eurjchem-1125	44	7	%	%	NOUN
eurjchem-1125	44	8	.	.	PUNCT
eurjchem-1125	45	1	m.p	m.p	PROPN
eurjchem-1125	45	2	.	.	PROPN
eurjchem-1125	45	3	:	:	PUNCT
eurjchem-1125	46	1	241	241	NUM
eurjchem-1125	46	2	°	°	ADP
eurjchem-1125	46	3	c	c	X
eurjchem-1125	46	4	.	.	PUNCT
eurjchem-1125	47	1	ft‐ir	ft‐ir	NOUN
eurjchem-1125	47	2	(	(	PUNCT
eurjchem-1125	47	3	kbr	kbr	PROPN
eurjchem-1125	47	4	,	,	PUNCT
eurjchem-1125	47	5	ν	ν	PROPN
eurjchem-1125	47	6	,	,	PUNCT
eurjchem-1125	47	7	cm‐1	cm‐1	PROPN
eurjchem-1125	47	8	):	):	PUNCT
eurjchem-1125	47	9	3415	3415	NUM
eurjchem-1125	47	10	,	,	PUNCT
eurjchem-1125	47	11	3305	3305	NUM
eurjchem-1125	47	12	,	,	PUNCT
eurjchem-1125	47	13	3261	3261	NUM
eurjchem-1125	47	14	(	(	PUNCT
eurjchem-1125	47	15	nh2	nh2	PROPN
eurjchem-1125	47	16	,	,	PUNCT
eurjchem-1125	47	17	nh	nh	PROPN
eurjchem-1125	47	18	)	)	PUNCT
eurjchem-1125	47	19	,	,	PUNCT
eurjchem-1125	47	20	1673	1673	NUM
eurjchem-1125	47	21	,	,	PUNCT
eurjchem-1125	47	22	1616	1616	NUM
eurjchem-1125	47	23	(	(	PUNCT
eurjchem-1125	47	24	c	c	NOUN
eurjchem-1125	47	25	=	=	NOUN
eurjchem-1125	47	26	o	o	NOUN
eurjchem-1125	47	27	)	)	PUNCT
eurjchem-1125	47	28	.	.	PUNCT
eurjchem-1125	48	1	1h	1h	NUM
eurjchem-1125	48	2	nmr	nmr	NOUN
eurjchem-1125	48	3	(	(	PUNCT
eurjchem-1125	48	4	400	400	NUM
eurjchem-1125	48	5	mhz	mhz	NOUN
eurjchem-1125	48	6	,	,	PUNCT
eurjchem-1125	48	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	48	8	,	,	PUNCT
eurjchem-1125	48	9	δ	δ	PROPN
eurjchem-1125	48	10	,	,	PUNCT
eurjchem-1125	48	11	ppm	ppm	NUM
eurjchem-1125	48	12	):	):	PUNCT
eurjchem-1125	48	13	1.30	1.30	NUM
eurjchem-1125	48	14	(	(	PUNCT
eurjchem-1125	48	15	t	t	PROPN
eurjchem-1125	48	16	,	,	PUNCT
eurjchem-1125	48	17	3h	3h	NUM
eurjchem-1125	48	18	,	,	PUNCT
eurjchem-1125	48	19	j	j	PROPN
eurjchem-1125	48	20	=	=	SYM
eurjchem-1125	48	21	6.8	6.8	NUM
eurjchem-1125	48	22	hz	hz	NOUN
eurjchem-1125	48	23	,	,	PUNCT
eurjchem-1125	48	24	ch3	ch3	PROPN
eurjchem-1125	48	25	)	)	PUNCT
eurjchem-1125	48	26	,	,	PUNCT
eurjchem-1125	48	27	1.71‐1.73	1.71‐1.73	NUM
eurjchem-1125	48	28	(	(	PUNCT
eurjchem-1125	48	29	m	m	PROPN
eurjchem-1125	48	30	,	,	PUNCT
eurjchem-1125	48	31	4h	4h	NOUN
eurjchem-1125	48	32	,	,	PUNCT
eurjchem-1125	48	33	c5‐2h	c5‐2h	PROPN
eurjchem-1125	48	34	,	,	PUNCT
eurjchem-1125	48	35	c6‐2h	c6‐2h	NOUN
eurjchem-1125	48	36	,	,	PUNCT
eurjchem-1125	48	37	cyclohexane	cyclohexane	NOUN
eurjchem-1125	48	38	skeleton	skeleton	NOUN
eurjchem-1125	48	39	)	)	PUNCT
eurjchem-1125	48	40	,	,	PUNCT
eurjchem-1125	48	41	2.37‐2.40	2.37‐2.40	NUM
eurjchem-1125	48	42	(	(	PUNCT
eurjchem-1125	48	43	m	m	PROPN
eurjchem-1125	48	44	,	,	PUNCT
eurjchem-1125	48	45	2h	2h	NUM
eurjchem-1125	48	46	,	,	PUNCT
eurjchem-1125	48	47	c5‐2h	c5‐2h	NOUN
eurjchem-1125	48	48	,	,	PUNCT
eurjchem-1125	48	49	cyclopentane	cyclopentane	ADJ
eurjchem-1125	48	50	skeleton	skeleton	NOUN
eurjchem-1125	48	51	)	)	PUNCT
eurjchem-1125	48	52	,	,	PUNCT
eurjchem-1125	48	53	2.58‐2.70	2.58‐2.70	NUM
eurjchem-1125	48	54	(	(	PUNCT
eurjchem-1125	48	55	m	m	PROPN
eurjchem-1125	48	56	,	,	PUNCT
eurjchem-1125	48	57	6h	6h	NUM
eurjchem-1125	48	58	,	,	PUNCT
eurjchem-1125	48	59	c4‐2h	c4‐2h	PROPN
eurjchem-1125	48	60	,	,	PUNCT
eurjchem-1125	48	61	c7‐2h	c7‐2h	PROPN
eurjchem-1125	48	62	,	,	PUNCT
eurjchem-1125	48	63	cyclohexane	cyclohexane	NOUN
eurjchem-1125	48	64	skeleton	skeleton	NOUN
eurjchem-1125	48	65	and	and	CCONJ
eurjchem-1125	48	66	c4‐	c4‐	ADV
eurjchem-1125	48	67	2h	2h	NUM
eurjchem-1125	48	68	,	,	PUNCT
eurjchem-1125	48	69	cyclopentane	cyclopentane	PROPN
eurjchem-1125	48	70	skeleton	skeleton	NOUN
eurjchem-1125	48	71	)	)	PUNCT
eurjchem-1125	48	72	,	,	PUNCT
eurjchem-1125	48	73	3.09‐3.18	3.09‐3.18	NUM
eurjchem-1125	48	74	(	(	PUNCT
eurjchem-1125	48	75	m	m	PROPN
eurjchem-1125	48	76	,	,	PUNCT
eurjchem-1125	48	77	2h	2h	NUM
eurjchem-1125	48	78	,	,	PUNCT
eurjchem-1125	48	79	c6‐2h	c6‐2h	NOUN
eurjchem-1125	48	80	,	,	PUNCT
eurjchem-1125	48	81	cyclopentane	cyclopentane	PROPN
eurjchem-1125	48	82	skeleton	skeleton	NOUN
eurjchem-1125	48	83	)	)	PUNCT
eurjchem-1125	48	84	,	,	PUNCT
eurjchem-1125	48	85	4.28	4.28	NUM
eurjchem-1125	48	86	(	(	PUNCT
eurjchem-1125	48	87	q	q	NOUN
eurjchem-1125	48	88	,	,	PUNCT
eurjchem-1125	48	89	2h	2h	NUM
eurjchem-1125	48	90	,	,	PUNCT
eurjchem-1125	48	91	j	j	PROPN
eurjchem-1125	48	92	=	=	SYM
eurjchem-1125	48	93	6.8	6.8	NUM
eurjchem-1125	48	94	hz	hz	NOUN
eurjchem-1125	48	95	,	,	PUNCT
eurjchem-1125	48	96	ch2o	ch2o	NOUN
eurjchem-1125	48	97	)	)	PUNCT
eurjchem-1125	48	98	,	,	PUNCT
eurjchem-1125	48	99	7.53	7.53	NUM
eurjchem-1125	48	100	(	(	PUNCT
eurjchem-1125	48	101	s	s	PROPN
eurjchem-1125	48	102	,	,	PUNCT
eurjchem-1125	48	103	2h	2h	NUM
eurjchem-1125	48	104	,	,	PUNCT
eurjchem-1125	48	105	nh2	nh2	PROPN
eurjchem-1125	48	106	)	)	PUNCT
eurjchem-1125	48	107	,	,	PUNCT
eurjchem-1125	48	108	11.04	11.04	NUM
eurjchem-1125	48	109	(	(	PUNCT
eurjchem-1125	48	110	s	s	PROPN
eurjchem-1125	48	111	,	,	PUNCT
eurjchem-1125	48	112	1h	1h	NUM
eurjchem-1125	48	113	,	,	PUNCT
eurjchem-1125	48	114	nh‐co	nh‐co	NUM
eurjchem-1125	48	115	)	)	PUNCT
eurjchem-1125	48	116	.	.	PUNCT
eurjchem-1125	49	1	13c	13c	NOUN
eurjchem-1125	49	2	nmr	nmr	NOUN
eurjchem-1125	49	3	(	(	PUNCT
eurjchem-1125	49	4	100	100	NUM
eurjchem-1125	49	5	mhz	mhz	NOUN
eurjchem-1125	49	6	,	,	PUNCT
eurjchem-1125	49	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	49	8	,	,	PUNCT
eurjchem-1125	49	9	δ	δ	PROPN
eurjchem-1125	49	10	,	,	PUNCT
eurjchem-1125	49	11	ppm	ppm	NOUN
eurjchem-1125	49	12	):	):	PUNCT
eurjchem-1125	49	13	168.7	168.7	NUM
eurjchem-1125	49	14	,	,	PUNCT
eurjchem-1125	49	15	165.3	165.3	NUM
eurjchem-1125	49	16	,	,	PUNCT
eurjchem-1125	49	17	161.3	161.3	NUM
eurjchem-1125	49	18	,	,	PUNCT
eurjchem-1125	49	19	147.0	147.0	NUM
eurjchem-1125	49	20	,	,	PUNCT
eurjchem-1125	49	21	137.6	137.6	NUM
eurjchem-1125	49	22	,	,	PUNCT
eurjchem-1125	49	23	129.8	129.8	NUM
eurjchem-1125	49	24	,	,	PUNCT
eurjchem-1125	49	25	125.3	125.3	NUM
eurjchem-1125	49	26	,	,	PUNCT
eurjchem-1125	49	27	120.3	120.3	NUM
eurjchem-1125	49	28	,	,	PUNCT
eurjchem-1125	49	29	110.0	110.0	NUM
eurjchem-1125	49	30	,	,	PUNCT
eurjchem-1125	49	31	100.9	100.9	NUM
eurjchem-1125	49	32	,	,	PUNCT
eurjchem-1125	49	33	59.9	59.9	NUM
eurjchem-1125	49	34	,	,	PUNCT
eurjchem-1125	49	35	29.28	29.28	NUM
eurjchem-1125	49	36	,	,	PUNCT
eurjchem-1125	49	37	25.7	25.7	NUM
eurjchem-1125	49	38	,	,	PUNCT
eurjchem-1125	49	39	23.4	23.4	NUM
eurjchem-1125	49	40	,	,	PUNCT
eurjchem-1125	49	41	22.3	22.3	NUM
eurjchem-1125	49	42	,	,	PUNCT
eurjchem-1125	49	43	22.2	22.2	NUM
eurjchem-1125	49	44	,	,	PUNCT
eurjchem-1125	49	45	13.8	13.8	NUM
eurjchem-1125	49	46	.	.	PUNCT
eurjchem-1125	50	1	ei‐ms	ei‐ms	PROPN
eurjchem-1125	50	2	(	(	PUNCT
eurjchem-1125	50	3	m	m	NOUN
eurjchem-1125	50	4	/	/	SYM
eurjchem-1125	50	5	z	z	NOUN
eurjchem-1125	50	6	(	(	PUNCT
eurjchem-1125	50	7	%	%	NOUN
eurjchem-1125	50	8	)	)	PUNCT
eurjchem-1125	50	9	):	):	PUNCT
eurjchem-1125	50	10	392	392	NUM
eurjchem-1125	50	11	(	(	PUNCT
eurjchem-1125	50	12	m++2	m++2	PROPN
eurjchem-1125	50	13	,	,	PUNCT
eurjchem-1125	50	14	3.13	3.13	NUM
eurjchem-1125	50	15	)	)	PUNCT
eurjchem-1125	50	16	,	,	PUNCT
eurjchem-1125	50	17	390	390	NUM
eurjchem-1125	50	18	(	(	PUNCT
eurjchem-1125	50	19	m+	m+	NUM
eurjchem-1125	50	20	,	,	PUNCT
eurjchem-1125	50	21	19.9	19.9	NUM
eurjchem-1125	50	22	)	)	PUNCT
eurjchem-1125	50	23	,	,	PUNCT
eurjchem-1125	50	24	344	344	NUM
eurjchem-1125	50	25	(	(	PUNCT
eurjchem-1125	50	26	3.3	3.3	NUM
eurjchem-1125	50	27	)	)	PUNCT
eurjchem-1125	50	28	,	,	PUNCT
eurjchem-1125	50	29	300	300	NUM
eurjchem-1125	50	30	(	(	PUNCT
eurjchem-1125	50	31	0.8	0.8	NUM
eurjchem-1125	50	32	)	)	PUNCT
eurjchem-1125	50	33	,	,	PUNCT
eurjchem-1125	50	34	225	225	NUM
eurjchem-1125	50	35	(	(	PUNCT
eurjchem-1125	50	36	62.9	62.9	NUM
eurjchem-1125	50	37	)	)	PUNCT
eurjchem-1125	50	38	,	,	PUNCT
eurjchem-1125	50	39	178	178	NUM
eurjchem-1125	50	40	(	(	PUNCT
eurjchem-1125	50	41	100	100	NUM
eurjchem-1125	50	42	)	)	PUNCT
eurjchem-1125	50	43	,	,	PUNCT
eurjchem-1125	50	44	166	166	NUM
eurjchem-1125	50	45	(	(	PUNCT
eurjchem-1125	50	46	73.0	73.0	NUM
eurjchem-1125	50	47	)	)	PUNCT
eurjchem-1125	50	48	,	,	PUNCT
eurjchem-1125	50	49	150	150	NUM
eurjchem-1125	50	50	(	(	PUNCT
eurjchem-1125	50	51	68.2	68.2	NUM
eurjchem-1125	50	52	)	)	PUNCT
eurjchem-1125	50	53	,	,	PUNCT
eurjchem-1125	50	54	138	138	NUM
eurjchem-1125	50	55	(	(	PUNCT
eurjchem-1125	50	56	26.7	26.7	NUM
eurjchem-1125	50	57	)	)	PUNCT
eurjchem-1125	50	58	,	,	PUNCT
eurjchem-1125	50	59	122	122	NUM
eurjchem-1125	50	60	(	(	PUNCT
eurjchem-1125	50	61	54.9	54.9	NUM
eurjchem-1125	50	62	)	)	PUNCT
eurjchem-1125	50	63	,	,	PUNCT
eurjchem-1125	50	64	109	109	NUM
eurjchem-1125	50	65	(	(	PUNCT
eurjchem-1125	50	66	65.9	65.9	NUM
eurjchem-1125	50	67	)	)	PUNCT
eurjchem-1125	50	68	,	,	PUNCT
eurjchem-1125	50	69	104	104	NUM
eurjchem-1125	50	70	(	(	PUNCT
eurjchem-1125	50	71	86.8	86.8	NUM
eurjchem-1125	50	72	)	)	PUNCT
eurjchem-1125	50	73	,	,	PUNCT
eurjchem-1125	50	74	90	90	NUM
eurjchem-1125	50	75	(	(	PUNCT
eurjchem-1125	50	76	32.2	32.2	NUM
eurjchem-1125	50	77	)	)	PUNCT
eurjchem-1125	50	78	,	,	PUNCT
eurjchem-1125	50	79	76	76	NUM
eurjchem-1125	50	80	(	(	PUNCT
eurjchem-1125	50	81	5.0	5.0	NUM
eurjchem-1125	50	82	)	)	PUNCT
eurjchem-1125	50	83	,	,	PUNCT
eurjchem-1125	50	84	65	65	NUM
eurjchem-1125	50	85	(	(	PUNCT
eurjchem-1125	50	86	48.2	48.2	NUM
eurjchem-1125	50	87	)	)	PUNCT
eurjchem-1125	50	88	.	.	PUNCT
eurjchem-1125	51	1	anal	anal	PROPN
eurjchem-1125	51	2	.	.	PUNCT
eurjchem-1125	51	3	calcd	calcd	NOUN
eurjchem-1125	51	4	.	.	PUNCT
eurjchem-1125	52	1	for	for	SCONJ
eurjchem-1125	52	2	c19h22n2o3s2	c19h22n2o3s2	NOUN
eurjchem-1125	52	3	:	:	PUNCT
eurjchem-1125	52	4	c	c	X
eurjchem-1125	52	5	,	,	PUNCT
eurjchem-1125	52	6	58.44	58.44	NUM
eurjchem-1125	52	7	;	;	PUNCT
eurjchem-1125	52	8	h	h	NOUN
eurjchem-1125	52	9	,	,	PUNCT
eurjchem-1125	52	10	5.68	5.68	NUM
eurjchem-1125	52	11	;	;	PUNCT
eurjchem-1125	52	12	n	n	CCONJ
eurjchem-1125	52	13	,	,	PUNCT
eurjchem-1125	52	14	7.17	7.17	NUM
eurjchem-1125	52	15	.	.	PUNCT
eurjchem-1125	52	16	found	find	VERB
eurjchem-1125	52	17	:	:	PUNCT
eurjchem-1125	53	1	c	c	X
eurjchem-1125	53	2	,	,	PUNCT
eurjchem-1125	53	3	58.40	58.40	NUM
eurjchem-1125	53	4	;	;	PUNCT
eurjchem-1125	53	5	h	h	X
eurjchem-1125	53	6	,	,	PUNCT
eurjchem-1125	53	7	5.64	5.64	NUM
eurjchem-1125	53	8	;	;	PUNCT
eurjchem-1125	53	9	n	n	CCONJ
eurjchem-1125	53	10	,	,	PUNCT
eurjchem-1125	53	11	7.14	7.14	NUM
eurjchem-1125	53	12	%	%	NOUN
eurjchem-1125	53	13	.	.	PUNCT
eurjchem-1125	54	1	ethyl	ethyl	PROPN
eurjchem-1125	54	2	2‐{[(2‐amino‐4	2‐{[(2‐amino‐4	NUM
eurjchem-1125	54	3	,	,	PUNCT
eurjchem-1125	54	4	5	5	NUM
eurjchem-1125	54	5	,	,	PUNCT
eurjchem-1125	54	6	6	6	NUM
eurjchem-1125	54	7	,	,	PUNCT
eurjchem-1125	54	8	7‐tetrahydro‐1‐benzothien‐3‐yl	7‐tetrahydro‐1‐benzothien‐3‐yl	NUM
eurjchem-1125	54	9	)	)	PUNCT
eurjchem-1125	55	1	carbonyl]amino}‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxy	carbonyl]amino}‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxy	ADJ
eurjchem-1125	55	2	late	late	ADV
eurjchem-1125	55	3	(	(	PUNCT
eurjchem-1125	55	4	5	5	NUM
eurjchem-1125	55	5	):	):	PUNCT
eurjchem-1125	55	6	color	color	NOUN
eurjchem-1125	55	7	:	:	PUNCT
eurjchem-1125	55	8	white	white	ADJ
eurjchem-1125	55	9	powder	powder	NOUN
eurjchem-1125	55	10	.	.	PUNCT
eurjchem-1125	56	1	yield	yield	NOUN
eurjchem-1125	56	2	:	:	PUNCT
eurjchem-1125	56	3	1.45	1.45	NUM
eurjchem-1125	56	4	g	g	NOUN
eurjchem-1125	56	5	,	,	PUNCT
eurjchem-1125	56	6	90	90	NUM
eurjchem-1125	56	7	%	%	NOUN
eurjchem-1125	56	8	.	.	PUNCT
eurjchem-1125	57	1	m.p	m.p	PROPN
eurjchem-1125	57	2	.	.	PROPN
eurjchem-1125	57	3	:	:	PUNCT
eurjchem-1125	58	1	200	200	NUM
eurjchem-1125	58	2	°	°	NOUN
eurjchem-1125	58	3	c	c	X
eurjchem-1125	58	4	.	.	PUNCT
eurjchem-1125	59	1	ft‐ir	ft‐ir	NOUN
eurjchem-1125	59	2	(	(	PUNCT
eurjchem-1125	59	3	kbr	kbr	PROPN
eurjchem-1125	59	4	,	,	PUNCT
eurjchem-1125	59	5	ν	ν	PROPN
eurjchem-1125	59	6	,	,	PUNCT
eurjchem-1125	59	7	cm‐1	cm‐1	PROPN
eurjchem-1125	59	8	):	):	PUNCT
eurjchem-1125	59	9	4421	4421	NUM
eurjchem-1125	59	10	,	,	PUNCT
eurjchem-1125	59	11	3397	3397	NUM
eurjchem-1125	59	12	,	,	PUNCT
eurjchem-1125	59	13	3299	3299	NUM
eurjchem-1125	59	14	(	(	PUNCT
eurjchem-1125	59	15	nh	nh	PROPN
eurjchem-1125	59	16	,	,	PUNCT
eurjchem-1125	59	17	nh2	nh2	PROPN
eurjchem-1125	59	18	)	)	PUNCT
eurjchem-1125	59	19	,	,	PUNCT
eurjchem-1125	59	20	1681	1681	NUM
eurjchem-1125	59	21	,	,	PUNCT
eurjchem-1125	59	22	1623	1623	NUM
eurjchem-1125	59	23	(	(	PUNCT
eurjchem-1125	59	24	c	c	NOUN
eurjchem-1125	59	25	=	=	NOUN
eurjchem-1125	59	26	o	o	NOUN
eurjchem-1125	59	27	)	)	PUNCT
eurjchem-1125	59	28	.	.	PUNCT
eurjchem-1125	60	1	1h	1h	NUM
eurjchem-1125	60	2	nmr	nmr	NOUN
eurjchem-1125	60	3	(	(	PUNCT
eurjchem-1125	60	4	400	400	NUM
eurjchem-1125	60	5	mhz	mhz	NOUN
eurjchem-1125	60	6	,	,	PUNCT
eurjchem-1125	60	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	60	8	,	,	PUNCT
eurjchem-1125	60	9	δ	δ	PROPN
eurjchem-1125	60	10	,	,	PUNCT
eurjchem-1125	60	11	ppm	ppm	NUM
eurjchem-1125	60	12	):	):	PUNCT
eurjchem-1125	60	13	1.30	1.30	NUM
eurjchem-1125	60	14	(	(	PUNCT
eurjchem-1125	60	15	t	t	PROPN
eurjchem-1125	60	16	,	,	PUNCT
eurjchem-1125	60	17	3h	3h	NUM
eurjchem-1125	60	18	,	,	PUNCT
eurjchem-1125	60	19	j	j	PROPN
eurjchem-1125	60	20	=	=	SYM
eurjchem-1125	60	21	6.8	6.8	NUM
eurjchem-1125	60	22	hz	hz	NOUN
eurjchem-1125	60	23	,	,	PUNCT
eurjchem-1125	60	24	ch3	ch3	PROPN
eurjchem-1125	60	25	)	)	PUNCT
eurjchem-1125	60	26	,	,	PUNCT
eurjchem-1125	60	27	1.73‐1.76	1.73‐1.76	NUM
eurjchem-1125	60	28	(	(	PUNCT
eurjchem-1125	60	29	m	m	PROPN
eurjchem-1125	60	30	,	,	PUNCT
eurjchem-1125	60	31	8h	8h	NUM
eurjchem-1125	60	32	,	,	PUNCT
eurjchem-1125	60	33	2c5‐2h	2c5‐2h	NUM
eurjchem-1125	60	34	,	,	PUNCT
eurjchem-1125	60	35	2c6‐2h	2c6‐2h	NUM
eurjchem-1125	60	36	,	,	PUNCT
eurjchem-1125	60	37	cyclohexane	cyclohexane	NOUN
eurjchem-1125	60	38	skeleton	skeleton	NOUN
eurjchem-1125	60	39	)	)	PUNCT
eurjchem-1125	60	40	,	,	PUNCT
eurjchem-1125	60	41	2.50‐2.59	2.50‐2.59	NUM
eurjchem-1125	60	42	(	(	PUNCT
eurjchem-1125	60	43	m	m	PROPN
eurjchem-1125	60	44	,	,	PUNCT
eurjchem-1125	60	45	4h	4h	NUM
eurjchem-1125	60	46	,	,	PUNCT
eurjchem-1125	60	47	2c4‐2h	2c4‐2h	NUM
eurjchem-1125	60	48	,	,	PUNCT
eurjchem-1125	60	49	cyclohexane	cyclohexane	NOUN
eurjchem-1125	60	50	skeleton	skeleton	NOUN
eurjchem-1125	60	51	)	)	PUNCT
eurjchem-1125	60	52	,	,	PUNCT
eurjchem-1125	60	53	2.72‐2.78	2.72‐2.78	PROPN
eurjchem-1125	60	54	(	(	PUNCT
eurjchem-1125	60	55	m	m	PROPN
eurjchem-1125	60	56	,	,	PUNCT
eurjchem-1125	60	57	4h	4h	NUM
eurjchem-1125	60	58	,	,	PUNCT
eurjchem-1125	60	59	2c7‐2h	2c7‐2h	NUM
eurjchem-1125	60	60	cyclohexane	cyclohexane	NOUN
eurjchem-1125	60	61	skeleton	skeleton	NOUN
eurjchem-1125	60	62	)	)	PUNCT
eurjchem-1125	60	63	,	,	PUNCT
eurjchem-1125	60	64	4.28	4.28	NUM
eurjchem-1125	60	65	(	(	PUNCT
eurjchem-1125	60	66	q	q	NOUN
eurjchem-1125	60	67	,	,	PUNCT
eurjchem-1125	60	68	2h	2h	NUM
eurjchem-1125	60	69	,	,	PUNCT
eurjchem-1125	60	70	j	j	PROPN
eurjchem-1125	60	71	=	=	SYM
eurjchem-1125	60	72	6.8	6.8	NUM
eurjchem-1125	60	73	hz	hz	NOUN
eurjchem-1125	60	74	,	,	PUNCT
eurjchem-1125	60	75	ch2o	ch2o	NOUN
eurjchem-1125	60	76	)	)	PUNCT
eurjchem-1125	60	77	,	,	PUNCT
eurjchem-1125	60	78	7.34	7.34	NUM
eurjchem-1125	60	79	(	(	PUNCT
eurjchem-1125	60	80	s	s	PROPN
eurjchem-1125	60	81	,	,	PUNCT
eurjchem-1125	60	82	2h	2h	NUM
eurjchem-1125	60	83	,	,	PUNCT
eurjchem-1125	60	84	nh2	nh2	PROPN
eurjchem-1125	60	85	)	)	PUNCT
eurjchem-1125	60	86	,	,	PUNCT
eurjchem-1125	60	87	11.10	11.10	NUM
eurjchem-1125	60	88	(	(	PUNCT
eurjchem-1125	60	89	s	s	PROPN
eurjchem-1125	60	90	,	,	PUNCT
eurjchem-1125	60	91	1h	1h	NUM
eurjchem-1125	60	92	,	,	PUNCT
eurjchem-1125	60	93	nh‐co	nh‐co	NUM
eurjchem-1125	60	94	)	)	PUNCT
eurjchem-1125	60	95	.	.	PUNCT
eurjchem-1125	61	1	13c	13c	NOUN
eurjchem-1125	61	2	nmr	nmr	NOUN
eurjchem-1125	61	3	(	(	PUNCT
eurjchem-1125	61	4	100	100	NUM
eurjchem-1125	61	5	mhz	mhz	NOUN
eurjchem-1125	61	6	,	,	PUNCT
eurjchem-1125	61	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	61	8	,	,	PUNCT
eurjchem-1125	61	9	δ	δ	PROPN
eurjchem-1125	61	10	,	,	PUNCT
eurjchem-1125	61	11	ppm	ppm	NOUN
eurjchem-1125	61	12	):	):	PUNCT
eurjchem-1125	61	13	165.1	165.1	NUM
eurjchem-1125	61	14	,	,	PUNCT
eurjchem-1125	61	15	162.4	162.4	NUM
eurjchem-1125	61	16	,	,	PUNCT
eurjchem-1125	61	17	161.6	161.6	NUM
eurjchem-1125	61	18	,	,	PUNCT
eurjchem-1125	61	19	147.0	147.0	NUM
eurjchem-1125	61	20	,	,	PUNCT
eurjchem-1125	61	21	129.9	129.9	NUM
eurjchem-1125	61	22	,	,	PUNCT
eurjchem-1125	61	23	128.3	128.3	NUM
eurjchem-1125	61	24	,	,	PUNCT
eurjchem-1125	61	25	125.3	125.3	NUM
eurjchem-1125	61	26	,	,	PUNCT
eurjchem-1125	61	27	116.6	116.6	NUM
eurjchem-1125	61	28	,	,	PUNCT
eurjchem-1125	61	29	110.1	110.1	NUM
eurjchem-1125	61	30	,	,	PUNCT
eurjchem-1125	61	31	105.1	105.1	NUM
eurjchem-1125	61	32	,	,	PUNCT
eurjchem-1125	61	33	59.8	59.8	NUM
eurjchem-1125	61	34	,	,	PUNCT
eurjchem-1125	61	35	25.9	25.9	NUM
eurjchem-1125	61	36	,	,	PUNCT
eurjchem-1125	61	37	25.7	25.7	NUM
eurjchem-1125	61	38	,	,	PUNCT
eurjchem-1125	61	39	22.3	22.3	NUM
eurjchem-1125	61	40	,	,	PUNCT
eurjchem-1125	61	41	22.2	22.2	NUM
eurjchem-1125	61	42	,	,	PUNCT
eurjchem-1125	61	43	13.8	13.8	NUM
eurjchem-1125	61	44	.	.	PUNCT
eurjchem-1125	62	1	ei‐ms	ei‐ms	PROPN
eurjchem-1125	62	2	(	(	PUNCT
eurjchem-1125	62	3	m	m	NOUN
eurjchem-1125	62	4	/	/	SYM
eurjchem-1125	62	5	z	z	NOUN
eurjchem-1125	62	6	(	(	PUNCT
eurjchem-1125	62	7	%	%	NOUN
eurjchem-1125	62	8	)	)	PUNCT
eurjchem-1125	62	9	):	):	PUNCT
eurjchem-1125	62	10	406	406	NUM
eurjchem-1125	62	11	(	(	PUNCT
eurjchem-1125	62	12	m++2	m++2	PROPN
eurjchem-1125	62	13	,	,	PUNCT
eurjchem-1125	62	14	2.0	2.0	NUM
eurjchem-1125	62	15	)	)	PUNCT
eurjchem-1125	62	16	,	,	PUNCT
eurjchem-1125	62	17	405	405	NUM
eurjchem-1125	62	18	(	(	PUNCT
eurjchem-1125	62	19	m++1	m++1	NOUN
eurjchem-1125	62	20	,	,	PUNCT
eurjchem-1125	62	21	4.47	4.47	NUM
eurjchem-1125	62	22	)	)	PUNCT
eurjchem-1125	62	23	,	,	PUNCT
eurjchem-1125	62	24	404	404	NUM
eurjchem-1125	62	25	(	(	PUNCT
eurjchem-1125	62	26	m+	m+	NUM
eurjchem-1125	62	27	,	,	PUNCT
eurjchem-1125	62	28	14.0	14.0	NUM
eurjchem-1125	62	29	)	)	PUNCT
eurjchem-1125	62	30	,	,	PUNCT
eurjchem-1125	62	31	325	325	NUM
eurjchem-1125	62	32	(	(	PUNCT
eurjchem-1125	62	33	3.4	3.4	NUM
eurjchem-1125	62	34	)	)	PUNCT
eurjchem-1125	62	35	,	,	PUNCT
eurjchem-1125	62	36	225	225	NUM
eurjchem-1125	62	37	(	(	PUNCT
eurjchem-1125	62	38	100	100	NUM
eurjchem-1125	62	39	)	)	PUNCT
eurjchem-1125	62	40	,	,	PUNCT
eurjchem-1125	62	41	180	180	NUM
eurjchem-1125	62	42	(	(	PUNCT
eurjchem-1125	62	43	67.2	67.2	NUM
eurjchem-1125	62	44	)	)	PUNCT
eurjchem-1125	62	45	,	,	PUNCT
eurjchem-1125	62	46	151	151	NUM
eurjchem-1125	62	47	(	(	PUNCT
eurjchem-1125	62	48	17.4	17.4	NUM
eurjchem-1125	62	49	)	)	PUNCT
eurjchem-1125	62	50	,	,	PUNCT
eurjchem-1125	62	51	91	91	NUM
eurjchem-1125	62	52	(	(	PUNCT
eurjchem-1125	62	53	15.5	15.5	NUM
eurjchem-1125	62	54	)	)	PUNCT
eurjchem-1125	62	55	,	,	PUNCT
eurjchem-1125	62	56	68	68	NUM
eurjchem-1125	62	57	(	(	PUNCT
eurjchem-1125	62	58	1.5	1.5	NUM
eurjchem-1125	62	59	)	)	PUNCT
eurjchem-1125	62	60	.	.	PUNCT
eurjchem-1125	63	1	anal	anal	PROPN
eurjchem-1125	63	2	.	.	PUNCT
eurjchem-1125	63	3	calcd	calcd	NOUN
eurjchem-1125	63	4	.	.	PUNCT
eurjchem-1125	64	1	for	for	ADP
eurjchem-1125	64	2	c20h24n2o3s2	c20h24n2o3s2	PRON
eurjchem-1125	64	3	:	:	PUNCT
eurjchem-1125	64	4	c	c	X
eurjchem-1125	64	5	,	,	PUNCT
eurjchem-1125	64	6	59.38	59.38	NUM
eurjchem-1125	64	7	;	;	PUNCT
eurjchem-1125	64	8	h	h	NOUN
eurjchem-1125	64	9	,	,	PUNCT
eurjchem-1125	64	10	5.98	5.98	NUM
eurjchem-1125	64	11	;	;	PUNCT
eurjchem-1125	64	12	n	n	CCONJ
eurjchem-1125	64	13	,	,	PUNCT
eurjchem-1125	64	14	6.92	6.92	NUM
eurjchem-1125	64	15	.	.	PUNCT
eurjchem-1125	64	16	found	find	VERB
eurjchem-1125	64	17	:	:	PUNCT
eurjchem-1125	65	1	c	c	X
eurjchem-1125	65	2	,	,	PUNCT
eurjchem-1125	65	3	59.43	59.43	NUM
eurjchem-1125	65	4	;	;	PUNCT
eurjchem-1125	65	5	h	h	NOUN
eurjchem-1125	65	6	,	,	PUNCT
eurjchem-1125	65	7	6.05	6.05	NUM
eurjchem-1125	65	8	;	;	PUNCT
eurjchem-1125	65	9	n	n	CCONJ
eurjchem-1125	65	10	,	,	PUNCT
eurjchem-1125	65	11	6.97	6.97	NUM
eurjchem-1125	65	12	%	%	NOUN
eurjchem-1125	65	13	.	.	PUNCT
eurjchem-1125	66	1	2.2.2	2.2.2	X
eurjchem-1125	66	2	.	.	PUNCT
eurjchem-1125	67	1	reaction	reaction	NOUN
eurjchem-1125	67	2	of	of	ADP
eurjchem-1125	67	3	2‐aminothiophene	2‐aminothiophene	ADJ
eurjchem-1125	67	4	derivatives	derivative	NOUN
eurjchem-1125	67	5	(	(	PUNCT
eurjchem-1125	67	6	4	4	NUM
eurjchem-1125	67	7	)	)	PUNCT
eurjchem-1125	67	8	or	or	CCONJ
eurjchem-1125	67	9	(	(	PUNCT
eurjchem-1125	67	10	5	5	NUM
eurjchem-1125	67	11	)	)	PUNCT
eurjchem-1125	67	12	with	with	ADP
eurjchem-1125	67	13	3‐(3,5‐dimethyl‐1h‐pyrazol‐1‐yl)‐3‐oxopropanenitrile	3‐(3,5‐dimethyl‐1h‐pyrazol‐1‐yl)‐3‐oxopropanenitrile	PROPN
eurjchem-1125	67	14	(	(	PUNCT
eurjchem-1125	67	15	2	2	NUM
eurjchem-1125	67	16	)	)	PUNCT
eurjchem-1125	67	17	general	general	ADJ
eurjchem-1125	67	18	procedure	procedure	NOUN
eurjchem-1125	67	19	:	:	PUNCT
eurjchem-1125	67	20	a	a	DET
eurjchem-1125	67	21	mixture	mixture	NOUN
eurjchem-1125	67	22	of	of	ADP
eurjchem-1125	67	23	compound	compound	NOUN
eurjchem-1125	67	24	4	4	NUM
eurjchem-1125	67	25	(	(	PUNCT
eurjchem-1125	67	26	5.40	5.40	NUM
eurjchem-1125	67	27	g	g	NOUN
eurjchem-1125	67	28	,	,	PUNCT
eurjchem-1125	67	29	14	14	NUM
eurjchem-1125	67	30	mmol	mmol	NOUN
eurjchem-1125	67	31	)	)	PUNCT
eurjchem-1125	67	32	or	or	CCONJ
eurjchem-1125	67	33	5	5	NUM
eurjchem-1125	67	34	(	(	PUNCT
eurjchem-1125	67	35	5.66	5.66	NUM
eurjchem-1125	67	36	g	g	NOUN
eurjchem-1125	67	37	,	,	PUNCT
eurjchem-1125	67	38	14	14	NUM
eurjchem-1125	67	39	mmol	mmol	NOUN
eurjchem-1125	67	40	)	)	PUNCT
eurjchem-1125	67	41	and	and	CCONJ
eurjchem-1125	67	42	compound	compound	VERB
eurjchem-1125	67	43	2	2	NUM
eurjchem-1125	68	1	[	[	X
eurjchem-1125	68	2	18	18	NUM
eurjchem-1125	68	3	]	]	PUNCT
eurjchem-1125	68	4	(	(	PUNCT
eurjchem-1125	68	5	2.28	2.28	NUM
eurjchem-1125	68	6	g	g	NOUN
eurjchem-1125	68	7	,	,	PUNCT
eurjchem-1125	68	8	14	14	NUM
eurjchem-1125	68	9	mmol	mmol	NOUN
eurjchem-1125	68	10	)	)	PUNCT
eurjchem-1125	68	11	in	in	ADP
eurjchem-1125	68	12	dioxane	dioxane	NOUN
eurjchem-1125	68	13	(	(	PUNCT
eurjchem-1125	68	14	20	20	NUM
eurjchem-1125	68	15	ml	ml	NOUN
eurjchem-1125	68	16	)	)	PUNCT
eurjchem-1125	68	17	,	,	PUNCT
eurjchem-1125	68	18	was	be	AUX
eurjchem-1125	68	19	refluxed	refluxe	VERB
eurjchem-1125	68	20	for	for	ADP
eurjchem-1125	68	21	5	5	NUM
eurjchem-1125	68	22	h.	h.	NOUN
eurjchem-1125	68	23	the	the	DET
eurjchem-1125	68	24	solvent	solvent	NOUN
eurjchem-1125	68	25	was	be	AUX
eurjchem-1125	68	26	evaporated	evaporate	VERB
eurjchem-1125	68	27	under	under	ADP
eurjchem-1125	68	28	vacuum	vacuum	NOUN
eurjchem-1125	68	29	and	and	CCONJ
eurjchem-1125	68	30	the	the	DET
eurjchem-1125	68	31	residue	residue	NOUN
eurjchem-1125	68	32	was	be	AUX
eurjchem-1125	68	33	crystallized	crystallize	VERB
eurjchem-1125	68	34	form	form	NOUN
eurjchem-1125	68	35	ethanol	ethanol	NOUN
eurjchem-1125	68	36	/	/	SYM
eurjchem-1125	68	37	dmf	dmf	PROPN
eurjchem-1125	68	38	(	(	PUNCT
eurjchem-1125	68	39	5:1	5:1	NUM
eurjchem-1125	68	40	,	,	PUNCT
eurjchem-1125	68	41	v	v	NOUN
eurjchem-1125	68	42	:	:	PUNCT
eurjchem-1125	68	43	v	v	NOUN
eurjchem-1125	68	44	)	)	PUNCT
eurjchem-1125	68	45	mixture	mixture	NOUN
eurjchem-1125	68	46	to	to	PART
eurjchem-1125	68	47	give	give	VERB
eurjchem-1125	68	48	compounds	compound	NOUN
eurjchem-1125	68	49	6	6	NUM
eurjchem-1125	68	50	and	and	CCONJ
eurjchem-1125	68	51	7	7	NUM
eurjchem-1125	68	52	,	,	PUNCT
eurjchem-1125	68	53	respectively	respectively	ADV
eurjchem-1125	68	54	(	(	PUNCT
eurjchem-1125	68	55	scheme	scheme	NOUN
eurjchem-1125	68	56	1	1	NUM
eurjchem-1125	68	57	)	)	PUNCT
eurjchem-1125	68	58	.	.	PUNCT
eurjchem-1125	69	1	ethyl	ethyl	PROPN
eurjchem-1125	69	2	2‐[({2‐[(cyanoacetyl)amino]‐5	2‐[({2‐[(cyanoacetyl)amino]‐5	NUM
eurjchem-1125	69	3	,	,	PUNCT
eurjchem-1125	69	4	6‐dihydro‐4h‐cyclo	6‐dihydro‐4h‐cyclo	NUM
eurjchem-1125	69	5	penta[b]thien‐3‐yl}carbonyl)amino]‐4,5,6,7‐tetrahydro‐1‐benzo	penta[b]thien‐3‐yl}carbonyl)amino]‐4,5,6,7‐tetrahydro‐1‐benzo	NUM
eurjchem-1125	69	6	thiophene‐3‐carboxylate	thiophene‐3‐carboxylate	NUM
eurjchem-1125	69	7	(	(	PUNCT
eurjchem-1125	69	8	6	6	NUM
eurjchem-1125	69	9	):	):	PUNCT
eurjchem-1125	69	10	color	color	NOUN
eurjchem-1125	69	11	:	:	PUNCT
eurjchem-1125	69	12	white	white	ADJ
eurjchem-1125	69	13	powder	powder	NOUN
eurjchem-1125	69	14	.	.	PUNCT
eurjchem-1125	69	15	yield	yield	NOUN
eurjchem-1125	69	16	:	:	PUNCT
eurjchem-1125	69	17	4.99	4.99	NUM
eurjchem-1125	69	18	g	g	NOUN
eurjchem-1125	69	19	,	,	PUNCT
eurjchem-1125	69	20	78	78	NUM
eurjchem-1125	69	21	%	%	NOUN
eurjchem-1125	69	22	.	.	PUNCT
eurjchem-1125	70	1	m.p	m.p	PROPN
eurjchem-1125	70	2	.	.	PROPN
eurjchem-1125	70	3	:	:	PUNCT
eurjchem-1125	71	1	227	227	NUM
eurjchem-1125	71	2	°	°	NUM
eurjchem-1125	71	3	c	c	X
eurjchem-1125	71	4	.	.	PUNCT
eurjchem-1125	72	1	ft‐ir	ft‐ir	NOUN
eurjchem-1125	72	2	(	(	PUNCT
eurjchem-1125	72	3	kbr	kbr	PROPN
eurjchem-1125	72	4	,	,	PUNCT
eurjchem-1125	72	5	ν	ν	PROPN
eurjchem-1125	72	6	,	,	PUNCT
eurjchem-1125	72	7	cm‐1	cm‐1	PROPN
eurjchem-1125	72	8	):	):	PUNCT
eurjchem-1125	72	9	3284	3284	NUM
eurjchem-1125	72	10	,	,	PUNCT
eurjchem-1125	72	11	3216	3216	NUM
eurjchem-1125	72	12	(	(	PUNCT
eurjchem-1125	72	13	nh	nh	NOUN
eurjchem-1125	72	14	)	)	PUNCT
eurjchem-1125	72	15	,	,	PUNCT
eurjchem-1125	72	16	2253	2253	NUM
eurjchem-1125	72	17	(	(	PUNCT
eurjchem-1125	72	18	cn	cn	PROPN
eurjchem-1125	72	19	)	)	PUNCT
eurjchem-1125	72	20	,	,	PUNCT
eurjchem-1125	72	21	1670	1670	NUM
eurjchem-1125	72	22	,	,	PUNCT
eurjchem-1125	72	23	1627	1627	NUM
eurjchem-1125	72	24	(	(	PUNCT
eurjchem-1125	72	25	c	c	NOUN
eurjchem-1125	72	26	=	=	NOUN
eurjchem-1125	72	27	o	o	NOUN
eurjchem-1125	72	28	)	)	PUNCT
eurjchem-1125	72	29	.	.	PUNCT
eurjchem-1125	73	1	1h	1h	NUM
eurjchem-1125	73	2	nmr	nmr	NOUN
eurjchem-1125	73	3	(	(	PUNCT
eurjchem-1125	73	4	400	400	NUM
eurjchem-1125	73	5	mhz	mhz	NOUN
eurjchem-1125	73	6	,	,	PUNCT
eurjchem-1125	73	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	73	8	,	,	PUNCT
eurjchem-1125	73	9	δ	δ	PROPN
eurjchem-1125	73	10	,	,	PUNCT
eurjchem-1125	73	11	ppm	ppm	NUM
eurjchem-1125	73	12	):	):	PUNCT
eurjchem-1125	73	13	1.32	1.32	NUM
eurjchem-1125	73	14	(	(	PUNCT
eurjchem-1125	73	15	t	t	PROPN
eurjchem-1125	73	16	,	,	PUNCT
eurjchem-1125	73	17	3h	3h	NUM
eurjchem-1125	73	18	,	,	PUNCT
eurjchem-1125	73	19	j	j	PROPN
eurjchem-1125	73	20	=	=	SYM
eurjchem-1125	73	21	7.2	7.2	NUM
eurjchem-1125	73	22	hz	hz	NOUN
eurjchem-1125	73	23	,	,	PUNCT
eurjchem-1125	73	24	ch3	ch3	PROPN
eurjchem-1125	73	25	)	)	PUNCT
eurjchem-1125	73	26	,	,	PUNCT
eurjchem-1125	73	27	1.72‐1.74	1.72‐1.74	NUM
eurjchem-1125	73	28	(	(	PUNCT
eurjchem-1125	73	29	m	m	PROPN
eurjchem-1125	73	30	,	,	PUNCT
eurjchem-1125	73	31	4h	4h	NOUN
eurjchem-1125	73	32	,	,	PUNCT
eurjchem-1125	73	33	c5‐2h	c5‐2h	PROPN
eurjchem-1125	73	34	,	,	PUNCT
eurjchem-1125	73	35	c6‐2h	c6‐2h	NOUN
eurjchem-1125	73	36	,	,	PUNCT
eurjchem-1125	73	37	cyclohexane	cyclohexane	NOUN
eurjchem-1125	73	38	skeleton	skeleton	NOUN
eurjchem-1125	73	39	)	)	PUNCT
eurjchem-1125	73	40	,	,	PUNCT
eurjchem-1125	73	41	2.44‐2.47	2.44‐2.47	NUM
eurjchem-1125	73	42	(	(	PUNCT
eurjchem-1125	73	43	m	m	PROPN
eurjchem-1125	73	44	,	,	PUNCT
eurjchem-1125	73	45	2h	2h	NUM
eurjchem-1125	73	46	,	,	PUNCT
eurjchem-1125	73	47	c5‐2h	c5‐2h	NOUN
eurjchem-1125	73	48	,	,	PUNCT
eurjchem-1125	73	49	cyclopentane	cyclopentane	ADJ
eurjchem-1125	73	50	skeleton	skeleton	NOUN
eurjchem-1125	73	51	)	)	PUNCT
eurjchem-1125	73	52	,	,	PUNCT
eurjchem-1125	73	53	2.63‐2.82	2.63‐2.82	NUM
eurjchem-1125	73	54	(	(	PUNCT
eurjchem-1125	73	55	m	m	PROPN
eurjchem-1125	73	56	,	,	PUNCT
eurjchem-1125	73	57	6h	6h	NUM
eurjchem-1125	73	58	,	,	PUNCT
eurjchem-1125	73	59	c4‐2h	c4‐2h	PROPN
eurjchem-1125	73	60	,	,	PUNCT
eurjchem-1125	73	61	c7‐2h	c7‐2h	PROPN
eurjchem-1125	73	62	,	,	PUNCT
eurjchem-1125	73	63	cyclohexane	cyclohexane	NOUN
eurjchem-1125	73	64	skeleton	skeleton	NOUN
eurjchem-1125	73	65	and	and	CCONJ
eurjchem-1125	73	66	c4‐2h	c4‐2h	NOUN
eurjchem-1125	73	67	,	,	PUNCT
eurjchem-1125	73	68	cyclopentane	cyclopentane	ADJ
eurjchem-1125	73	69	skeleton	skeleton	NOUN
eurjchem-1125	73	70	)	)	PUNCT
eurjchem-1125	73	71	,	,	PUNCT
eurjchem-1125	73	72	3.09‐3.20	3.09‐3.20	NUM
eurjchem-1125	73	73	(	(	PUNCT
eurjchem-1125	73	74	m	m	PROPN
eurjchem-1125	73	75	,	,	PUNCT
eurjchem-1125	73	76	2h	2h	NUM
eurjchem-1125	73	77	,	,	PUNCT
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eurjchem-1125	73	79	,	,	PUNCT
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eurjchem-1125	73	82	)	)	PUNCT
eurjchem-1125	73	83	,	,	PUNCT
eurjchem-1125	73	84	4.23	4.23	NUM
eurjchem-1125	73	85	(	(	PUNCT
eurjchem-1125	73	86	s	s	PROPN
eurjchem-1125	73	87	,	,	PUNCT
eurjchem-1125	73	88	2h	2h	NUM
eurjchem-1125	73	89	,	,	PUNCT
eurjchem-1125	73	90	ch2cn	ch2cn	NUM
eurjchem-1125	73	91	)	)	PUNCT
eurjchem-1125	73	92	,	,	PUNCT
eurjchem-1125	73	93	4.30	4.30	NUM
eurjchem-1125	73	94	(	(	PUNCT
eurjchem-1125	73	95	q	q	NOUN
eurjchem-1125	73	96	,	,	PUNCT
eurjchem-1125	73	97	2h	2h	NUM
eurjchem-1125	73	98	,	,	PUNCT
eurjchem-1125	73	99	j	j	PROPN
eurjchem-1125	73	100	=	=	SYM
eurjchem-1125	73	101	7.2	7.2	NUM
eurjchem-1125	73	102	hz	hz	NOUN
eurjchem-1125	73	103	,	,	PUNCT
eurjchem-1125	73	104	ch2o	ch2o	NOUN
eurjchem-1125	73	105	)	)	PUNCT
eurjchem-1125	73	106	,	,	PUNCT
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eurjchem-1125	73	108	(	(	PUNCT
eurjchem-1125	73	109	s	s	PROPN
eurjchem-1125	73	110	,	,	PUNCT
eurjchem-1125	73	111	1h	1h	NUM
eurjchem-1125	73	112	,	,	PUNCT
eurjchem-1125	73	113	nh‐co	nh‐co	NUM
eurjchem-1125	73	114	)	)	PUNCT
eurjchem-1125	73	115	,	,	PUNCT
eurjchem-1125	73	116	11.64	11.64	NUM
eurjchem-1125	73	117	(	(	PUNCT
eurjchem-1125	73	118	s	s	PROPN
eurjchem-1125	73	119	,	,	PUNCT
eurjchem-1125	73	120	1h	1h	NUM
eurjchem-1125	73	121	,	,	PUNCT
eurjchem-1125	73	122	nh‐co	nh‐co	NUM
eurjchem-1125	73	123	)	)	PUNCT
eurjchem-1125	73	124	.	.	PUNCT
eurjchem-1125	74	1	13c	13c	NOUN
eurjchem-1125	74	2	nmr	nmr	NOUN
eurjchem-1125	74	3	(	(	PUNCT
eurjchem-1125	74	4	100	100	NUM
eurjchem-1125	74	5	mhz	mhz	NOUN
eurjchem-1125	74	6	,	,	PUNCT
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eurjchem-1125	74	8	,	,	PUNCT
eurjchem-1125	74	9	δ	δ	PROPN
eurjchem-1125	74	10	,	,	PUNCT
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eurjchem-1125	74	12	):	):	PUNCT
eurjchem-1125	74	13	166.2	166.2	NUM
eurjchem-1125	74	14	,	,	PUNCT
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eurjchem-1125	74	16	,	,	PUNCT
eurjchem-1125	74	17	149.1	149.1	NUM
eurjchem-1125	74	18	,	,	PUNCT
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eurjchem-1125	74	20	,	,	PUNCT
eurjchem-1125	74	21	137.8	137.8	NUM
eurjchem-1125	74	22	,	,	PUNCT
eurjchem-1125	74	23	134.0	134.0	NUM
eurjchem-1125	74	24	,	,	PUNCT
eurjchem-1125	74	25	130.4	130.4	NUM
eurjchem-1125	74	26	,	,	PUNCT
eurjchem-1125	74	27	126.7	126.7	NUM
eurjchem-1125	74	28	,	,	PUNCT
eurjchem-1125	74	29	116.0	116.0	NUM
eurjchem-1125	74	30	,	,	PUNCT
eurjchem-1125	74	31	112.2	112.2	NUM
eurjchem-1125	74	32	,	,	PUNCT
eurjchem-1125	74	33	111.1	111.1	NUM
eurjchem-1125	74	34	,	,	PUNCT
eurjchem-1125	74	35	60.3	60.3	NUM
eurjchem-1125	74	36	,	,	PUNCT
eurjchem-1125	74	37	29.0	29.0	NUM
eurjchem-1125	74	38	,	,	PUNCT
eurjchem-1125	74	39	28.0	28.0	NUM
eurjchem-1125	74	40	,	,	PUNCT
eurjchem-1125	74	41	27.6	27.6	NUM
eurjchem-1125	74	42	,	,	PUNCT
eurjchem-1125	74	43	25.7	25.7	NUM
eurjchem-1125	74	44	,	,	PUNCT
eurjchem-1125	74	45	23.5	23.5	NUM
eurjchem-1125	74	46	,	,	PUNCT
eurjchem-1125	74	47	22.2	22.2	NUM
eurjchem-1125	74	48	,	,	PUNCT
eurjchem-1125	74	49	22.1	22.1	NUM
eurjchem-1125	74	50	,	,	PUNCT
eurjchem-1125	74	51	13.8	13.8	NUM
eurjchem-1125	74	52	.	.	PUNCT
eurjchem-1125	75	1	ei‐ms	ei‐ms	PROPN
eurjchem-1125	75	2	(	(	PUNCT
eurjchem-1125	75	3	m	m	NOUN
eurjchem-1125	75	4	/	/	SYM
eurjchem-1125	75	5	z	z	NOUN
eurjchem-1125	75	6	(	(	PUNCT
eurjchem-1125	75	7	%	%	NOUN
eurjchem-1125	75	8	)	)	PUNCT
eurjchem-1125	75	9	):	):	PUNCT
eurjchem-1125	75	10	459	459	NUM
eurjchem-1125	75	11	(	(	PUNCT
eurjchem-1125	75	12	m++2	m++2	PROPN
eurjchem-1125	75	13	,	,	PUNCT
eurjchem-1125	75	14	0.6	0.6	NUM
eurjchem-1125	75	15	)	)	PUNCT
eurjchem-1125	75	16	,	,	PUNCT
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eurjchem-1125	75	18	(	(	PUNCT
eurjchem-1125	75	19	m+	m+	NUM
eurjchem-1125	75	20	,	,	PUNCT
eurjchem-1125	75	21	1.5	1.5	NUM
eurjchem-1125	75	22	)	)	PUNCT
eurjchem-1125	75	23	,	,	PUNCT
eurjchem-1125	75	24	295	295	NUM
eurjchem-1125	75	25	(	(	PUNCT
eurjchem-1125	75	26	0.3	0.3	NUM
eurjchem-1125	75	27	)	)	PUNCT
eurjchem-1125	75	28	,	,	PUNCT
eurjchem-1125	75	29	251	251	NUM
eurjchem-1125	75	30	(	(	PUNCT
eurjchem-1125	75	31	0.6	0.6	NUM
eurjchem-1125	75	32	)	)	PUNCT
eurjchem-1125	75	33	,	,	PUNCT
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eurjchem-1125	75	35	(	(	PUNCT
eurjchem-1125	75	36	12.3	12.3	NUM
eurjchem-1125	75	37	)	)	PUNCT
eurjchem-1125	75	38	,	,	PUNCT
eurjchem-1125	75	39	225	225	NUM
eurjchem-1125	75	40	(	(	PUNCT
eurjchem-1125	75	41	26.8	26.8	NUM
eurjchem-1125	75	42	)	)	PUNCT
eurjchem-1125	75	43	,	,	PUNCT
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eurjchem-1125	75	45	(	(	PUNCT
eurjchem-1125	75	46	5.4	5.4	NUM
eurjchem-1125	75	47	)	)	PUNCT
eurjchem-1125	75	48	,	,	PUNCT
eurjchem-1125	75	49	178	178	NUM
eurjchem-1125	75	50	(	(	PUNCT
eurjchem-1125	75	51	37.6	37.6	NUM
eurjchem-1125	75	52	)	)	PUNCT
eurjchem-1125	75	53	,	,	PUNCT
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eurjchem-1125	75	55	(	(	PUNCT
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eurjchem-1125	75	57	)	)	PUNCT
eurjchem-1125	75	58	,	,	PUNCT
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eurjchem-1125	75	60	(	(	PUNCT
eurjchem-1125	75	61	17.1	17.1	NUM
eurjchem-1125	75	62	)	)	PUNCT
eurjchem-1125	75	63	,	,	PUNCT
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eurjchem-1125	75	65	(	(	PUNCT
eurjchem-1125	75	66	13.9	13.9	NUM
eurjchem-1125	75	67	)	)	PUNCT
eurjchem-1125	75	68	,	,	PUNCT
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eurjchem-1125	75	70	(	(	PUNCT
eurjchem-1125	75	71	9.7	9.7	NUM
eurjchem-1125	75	72	)	)	PUNCT
eurjchem-1125	75	73	,	,	PUNCT
eurjchem-1125	75	74	67	67	NUM
eurjchem-1125	75	75	(	(	PUNCT
eurjchem-1125	75	76	100	100	NUM
eurjchem-1125	75	77	)	)	PUNCT
eurjchem-1125	75	78	.	.	PUNCT
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eurjchem-1125	76	2	.	.	PUNCT
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eurjchem-1125	76	4	.	.	PUNCT
eurjchem-1125	77	1	for	for	SCONJ
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eurjchem-1125	77	3	:	:	PUNCT
eurjchem-1125	77	4	c	c	X
eurjchem-1125	77	5	,	,	PUNCT
eurjchem-1125	77	6	57.75	57.75	NUM
eurjchem-1125	77	7	;	;	PUNCT
eurjchem-1125	77	8	h	h	NOUN
eurjchem-1125	77	9	,	,	PUNCT
eurjchem-1125	77	10	5.07	5.07	NUM
eurjchem-1125	77	11	;	;	PUNCT
eurjchem-1125	77	12	n	n	CCONJ
eurjchem-1125	77	13	,	,	PUNCT
eurjchem-1125	77	14	9.18	9.18	NUM
eurjchem-1125	77	15	.	.	PUNCT
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eurjchem-1125	77	17	:	:	PUNCT
eurjchem-1125	78	1	c	c	X
eurjchem-1125	78	2	,	,	PUNCT
eurjchem-1125	78	3	57.53	57.53	NUM
eurjchem-1125	78	4	;	;	PUNCT
eurjchem-1125	78	5	h	h	NOUN
eurjchem-1125	78	6	,	,	PUNCT
eurjchem-1125	78	7	5.01	5.01	NUM
eurjchem-1125	78	8	;	;	PUNCT
eurjchem-1125	78	9	n	n	CCONJ
eurjchem-1125	78	10	,	,	PUNCT
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eurjchem-1125	78	13	.	.	PUNCT
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eurjchem-1125	79	3	and	and	CCONJ
eurjchem-1125	79	4	el‐bialy	el‐bialy	PROPN
eurjchem-1125	79	5	/	/	SYM
eurjchem-1125	79	6	european	european	PROPN
eurjchem-1125	79	7	journal	journal	PROPN
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eurjchem-1125	79	10	5	5	NUM
eurjchem-1125	79	11	(	(	PUNCT
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eurjchem-1125	79	13	)	)	PUNCT
eurjchem-1125	79	14	(	(	PUNCT
eurjchem-1125	79	15	2014	2014	NUM
eurjchem-1125	79	16	)	)	PUNCT
eurjchem-1125	79	17	644‐651	644‐651	NUM
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eurjchem-1125	79	19	2	2	NUM
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eurjchem-1125	79	22	,	,	PUNCT
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eurjchem-1125	79	24	,	,	PUNCT
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eurjchem-1125	79	26	,	,	PUNCT
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eurjchem-1125	79	30	,	,	PUNCT
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eurjchem-1125	79	37	(	(	PUNCT
eurjchem-1125	79	38	7	7	NUM
eurjchem-1125	79	39	):	):	PUNCT
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eurjchem-1125	79	41	:	:	PUNCT
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eurjchem-1125	79	44	.	.	PUNCT
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eurjchem-1125	80	2	:	:	PUNCT
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eurjchem-1125	80	4	g	g	NOUN
eurjchem-1125	80	5	,	,	PUNCT
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eurjchem-1125	80	8	.	.	PUNCT
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eurjchem-1125	81	2	.	.	PROPN
eurjchem-1125	81	3	:	:	PUNCT
eurjchem-1125	82	1	237	237	NUM
eurjchem-1125	82	2	°	°	SYM
eurjchem-1125	82	3	c	c	X
eurjchem-1125	82	4	.	.	PUNCT
eurjchem-1125	83	1	ft‐ir	ft‐ir	NOUN
eurjchem-1125	83	2	(	(	PUNCT
eurjchem-1125	83	3	kbr	kbr	PROPN
eurjchem-1125	83	4	,	,	PUNCT
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eurjchem-1125	83	6	,	,	PUNCT
eurjchem-1125	83	7	cm‐1	cm‐1	PROPN
eurjchem-1125	83	8	):	):	PUNCT
eurjchem-1125	83	9	3293	3293	NUM
eurjchem-1125	83	10	,	,	PUNCT
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eurjchem-1125	83	12	(	(	PUNCT
eurjchem-1125	83	13	nh	nh	NOUN
eurjchem-1125	83	14	)	)	PUNCT
eurjchem-1125	83	15	,	,	PUNCT
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eurjchem-1125	83	17	(	(	PUNCT
eurjchem-1125	83	18	cn	cn	PROPN
eurjchem-1125	83	19	)	)	PUNCT
eurjchem-1125	83	20	,	,	PUNCT
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eurjchem-1125	83	22	,	,	PUNCT
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eurjchem-1125	83	25	c	c	NOUN
eurjchem-1125	83	26	=	=	NOUN
eurjchem-1125	83	27	o	o	NOUN
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eurjchem-1125	83	29	.	.	PUNCT
eurjchem-1125	84	1	1h	1h	NUM
eurjchem-1125	84	2	nmr	nmr	NOUN
eurjchem-1125	84	3	(	(	PUNCT
eurjchem-1125	84	4	400	400	NUM
eurjchem-1125	84	5	mhz	mhz	NOUN
eurjchem-1125	84	6	,	,	PUNCT
eurjchem-1125	84	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	84	8	,	,	PUNCT
eurjchem-1125	84	9	δ	δ	PROPN
eurjchem-1125	84	10	,	,	PUNCT
eurjchem-1125	84	11	ppm	ppm	NOUN
eurjchem-1125	84	12	):	):	PUNCT
eurjchem-1125	84	13	1.31	1.31	NUM
eurjchem-1125	84	14	(	(	PUNCT
eurjchem-1125	84	15	t	t	PROPN
eurjchem-1125	84	16	,	,	PUNCT
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eurjchem-1125	84	20	=	=	SYM
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eurjchem-1125	84	22	hz	hz	NOUN
eurjchem-1125	84	23	,	,	PUNCT
eurjchem-1125	84	24	ch3	ch3	PROPN
eurjchem-1125	84	25	)	)	PUNCT
eurjchem-1125	84	26	,	,	PUNCT
eurjchem-1125	84	27	1.74‐1.80	1.74‐1.80	NUM
eurjchem-1125	84	28	(	(	PUNCT
eurjchem-1125	84	29	m	m	PROPN
eurjchem-1125	84	30	,	,	PUNCT
eurjchem-1125	84	31	8h	8h	NUM
eurjchem-1125	84	32	,	,	PUNCT
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eurjchem-1125	84	34	,	,	PUNCT
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eurjchem-1125	84	36	,	,	PUNCT
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eurjchem-1125	84	40	,	,	PUNCT
eurjchem-1125	84	41	2.62‐2.80	2.62‐2.80	NUM
eurjchem-1125	84	42	(	(	PUNCT
eurjchem-1125	84	43	m	m	PROPN
eurjchem-1125	84	44	,	,	PUNCT
eurjchem-1125	84	45	8h	8h	NUM
eurjchem-1125	84	46	,	,	PUNCT
eurjchem-1125	84	47	2c4‐2h	2c4‐2h	NUM
eurjchem-1125	84	48	,	,	PUNCT
eurjchem-1125	84	49	2c7‐2h	2c7‐2h	NUM
eurjchem-1125	84	50	cyclohexane	cyclohexane	NOUN
eurjchem-1125	84	51	skeleton	skeleton	NOUN
eurjchem-1125	84	52	)	)	PUNCT
eurjchem-1125	84	53	,	,	PUNCT
eurjchem-1125	84	54	4.08	4.08	NUM
eurjchem-1125	84	55	(	(	PUNCT
eurjchem-1125	84	56	s	s	PROPN
eurjchem-1125	84	57	,	,	PUNCT
eurjchem-1125	84	58	2h	2h	NUM
eurjchem-1125	84	59	,	,	PUNCT
eurjchem-1125	84	60	ch2cn	ch2cn	NUM
eurjchem-1125	84	61	)	)	PUNCT
eurjchem-1125	84	62	,	,	PUNCT
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eurjchem-1125	84	64	(	(	PUNCT
eurjchem-1125	84	65	q	q	NOUN
eurjchem-1125	84	66	,	,	PUNCT
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eurjchem-1125	84	68	,	,	PUNCT
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eurjchem-1125	84	70	=	=	SYM
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eurjchem-1125	84	72	hz	hz	NOUN
eurjchem-1125	84	73	,	,	PUNCT
eurjchem-1125	84	74	ch2o	ch2o	NOUN
eurjchem-1125	84	75	)	)	PUNCT
eurjchem-1125	84	76	,	,	PUNCT
eurjchem-1125	84	77	11.37	11.37	NUM
eurjchem-1125	84	78	(	(	PUNCT
eurjchem-1125	84	79	s	s	PROPN
eurjchem-1125	84	80	,	,	PUNCT
eurjchem-1125	84	81	1h	1h	NUM
eurjchem-1125	84	82	,	,	PUNCT
eurjchem-1125	84	83	nh‐co	nh‐co	NUM
eurjchem-1125	84	84	)	)	PUNCT
eurjchem-1125	84	85	,	,	PUNCT
eurjchem-1125	84	86	11.46	11.46	NUM
eurjchem-1125	84	87	(	(	PUNCT
eurjchem-1125	84	88	s	s	PROPN
eurjchem-1125	84	89	,	,	PUNCT
eurjchem-1125	84	90	1h	1h	NUM
eurjchem-1125	84	91	,	,	PUNCT
eurjchem-1125	84	92	nh‐co	nh‐co	NUM
eurjchem-1125	84	93	)	)	PUNCT
eurjchem-1125	84	94	.	.	PUNCT
eurjchem-1125	85	1	13c	13c	NOUN
eurjchem-1125	85	2	nmr	nmr	NOUN
eurjchem-1125	85	3	(	(	PUNCT
eurjchem-1125	85	4	100	100	NUM
eurjchem-1125	85	5	mhz	mhz	NOUN
eurjchem-1125	85	6	,	,	PUNCT
eurjchem-1125	85	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	85	8	,	,	PUNCT
eurjchem-1125	85	9	δ	δ	PROPN
eurjchem-1125	85	10	,	,	PUNCT
eurjchem-1125	85	11	ppm	ppm	NOUN
eurjchem-1125	85	12	):	):	PUNCT
eurjchem-1125	85	13	165.3	165.3	NUM
eurjchem-1125	85	14	,	,	PUNCT
eurjchem-1125	85	15	160.8	160.8	NUM
eurjchem-1125	85	16	,	,	PUNCT
eurjchem-1125	85	17	160.3	160.3	NUM
eurjchem-1125	85	18	,	,	PUNCT
eurjchem-1125	85	19	145.7	145.7	NUM
eurjchem-1125	85	20	,	,	PUNCT
eurjchem-1125	85	21	130.4	130.4	NUM
eurjchem-1125	85	22	,	,	PUNCT
eurjchem-1125	85	23	129.2	129.2	NUM
eurjchem-1125	85	24	,	,	PUNCT
eurjchem-1125	85	25	128.4	128.4	NUM
eurjchem-1125	85	26	,	,	PUNCT
eurjchem-1125	85	27	126.4	126.4	NUM
eurjchem-1125	85	28	,	,	PUNCT
eurjchem-1125	85	29	117.3	117.3	NUM
eurjchem-1125	85	30	,	,	PUNCT
eurjchem-1125	85	31	115.0	115.0	NUM
eurjchem-1125	85	32	,	,	PUNCT
eurjchem-1125	85	33	111.7	111.7	NUM
eurjchem-1125	85	34	,	,	PUNCT
eurjchem-1125	85	35	60.2	60.2	NUM
eurjchem-1125	85	36	,	,	PUNCT
eurjchem-1125	85	37	25.8	25.8	NUM
eurjchem-1125	85	38	,	,	PUNCT
eurjchem-1125	85	39	23.6	23.6	NUM
eurjchem-1125	85	40	,	,	PUNCT
eurjchem-1125	85	41	23.5	23.5	NUM
eurjchem-1125	85	42	,	,	PUNCT
eurjchem-1125	85	43	22.2	22.2	NUM
eurjchem-1125	85	44	,	,	PUNCT
eurjchem-1125	85	45	22.1	22.1	NUM
eurjchem-1125	85	46	,	,	PUNCT
eurjchem-1125	85	47	22.0	22.0	NUM
eurjchem-1125	85	48	,	,	PUNCT
eurjchem-1125	85	49	13.8	13.8	NUM
eurjchem-1125	85	50	.	.	PUNCT
eurjchem-1125	86	1	ei‐ms	ei‐ms	PROPN
eurjchem-1125	86	2	(	(	PUNCT
eurjchem-1125	86	3	m	m	NOUN
eurjchem-1125	86	4	/	/	SYM
eurjchem-1125	86	5	z	z	NOUN
eurjchem-1125	86	6	(	(	PUNCT
eurjchem-1125	86	7	%	%	NOUN
eurjchem-1125	86	8	)	)	PUNCT
eurjchem-1125	86	9	):	):	PUNCT
eurjchem-1125	86	10	473	473	NUM
eurjchem-1125	86	11	(	(	PUNCT
eurjchem-1125	86	12	m++2	m++2	PROPN
eurjchem-1125	86	13	,	,	PUNCT
eurjchem-1125	86	14	0.8	0.8	NUM
eurjchem-1125	86	15	)	)	PUNCT
eurjchem-1125	86	16	,	,	PUNCT
eurjchem-1125	86	17	471	471	NUM
eurjchem-1125	86	18	(	(	PUNCT
eurjchem-1125	86	19	m+	m+	NUM
eurjchem-1125	86	20	,	,	PUNCT
eurjchem-1125	86	21	7.2	7.2	NUM
eurjchem-1125	86	22	)	)	PUNCT
eurjchem-1125	86	23	,	,	PUNCT
eurjchem-1125	86	24	247	247	NUM
eurjchem-1125	86	25	(	(	PUNCT
eurjchem-1125	86	26	8.6	8.6	NUM
eurjchem-1125	86	27	)	)	PUNCT
eurjchem-1125	86	28	,	,	PUNCT
eurjchem-1125	86	29	225	225	NUM
eurjchem-1125	86	30	(	(	PUNCT
eurjchem-1125	86	31	100	100	NUM
eurjchem-1125	86	32	)	)	PUNCT
eurjchem-1125	86	33	,	,	PUNCT
eurjchem-1125	86	34	206	206	NUM
eurjchem-1125	86	35	(	(	PUNCT
eurjchem-1125	86	36	10.3	10.3	NUM
eurjchem-1125	86	37	)	)	PUNCT
eurjchem-1125	86	38	,	,	PUNCT
eurjchem-1125	86	39	179	179	NUM
eurjchem-1125	86	40	(	(	PUNCT
eurjchem-1125	86	41	52.8	52.8	NUM
eurjchem-1125	86	42	)	)	PUNCT
eurjchem-1125	86	43	,	,	PUNCT
eurjchem-1125	86	44	151	151	NUM
eurjchem-1125	86	45	(	(	PUNCT
eurjchem-1125	86	46	21.4	21.4	NUM
eurjchem-1125	86	47	)	)	PUNCT
eurjchem-1125	86	48	,	,	PUNCT
eurjchem-1125	86	49	91	91	NUM
eurjchem-1125	86	50	(	(	PUNCT
eurjchem-1125	86	51	13.3	13.3	NUM
eurjchem-1125	86	52	)	)	PUNCT
eurjchem-1125	86	53	,	,	PUNCT
eurjchem-1125	86	54	68	68	NUM
eurjchem-1125	86	55	(	(	PUNCT
eurjchem-1125	86	56	50.5	50.5	NUM
eurjchem-1125	86	57	)	)	PUNCT
eurjchem-1125	86	58	.	.	PUNCT
eurjchem-1125	87	1	anal	anal	PROPN
eurjchem-1125	87	2	.	.	PUNCT
eurjchem-1125	87	3	calcd	calcd	NOUN
eurjchem-1125	87	4	.	.	PUNCT
eurjchem-1125	88	1	for	for	ADP
eurjchem-1125	88	2	c23h25n3o4s2	c23h25n3o4s2	NOUN
eurjchem-1125	88	3	:	:	PUNCT
eurjchem-1125	88	4	c	c	X
eurjchem-1125	88	5	,	,	PUNCT
eurjchem-1125	88	6	58.58	58.58	NUM
eurjchem-1125	88	7	;	;	PUNCT
eurjchem-1125	88	8	h	h	NOUN
eurjchem-1125	88	9	,	,	PUNCT
eurjchem-1125	88	10	5.34	5.34	NUM
eurjchem-1125	88	11	;	;	PUNCT
eurjchem-1125	88	12	n	n	CCONJ
eurjchem-1125	88	13	,	,	PUNCT
eurjchem-1125	88	14	8.91	8.91	NUM
eurjchem-1125	88	15	.	.	PUNCT
eurjchem-1125	88	16	found	find	VERB
eurjchem-1125	88	17	:	:	PUNCT
eurjchem-1125	89	1	c	c	X
eurjchem-1125	89	2	,	,	PUNCT
eurjchem-1125	89	3	58.53	58.53	NUM
eurjchem-1125	89	4	;	;	PUNCT
eurjchem-1125	89	5	h	h	NOUN
eurjchem-1125	89	6	,	,	PUNCT
eurjchem-1125	89	7	5.30	5.30	NUM
eurjchem-1125	89	8	;	;	PUNCT
eurjchem-1125	89	9	n	n	CCONJ
eurjchem-1125	89	10	,	,	PUNCT
eurjchem-1125	89	11	8.87	8.87	NUM
eurjchem-1125	89	12	%	%	NOUN
eurjchem-1125	89	13	.	.	PUNCT
eurjchem-1125	90	1	2.2.3	2.2.3	X
eurjchem-1125	90	2	.	.	PUNCT
eurjchem-1125	91	1	reaction	reaction	NOUN
eurjchem-1125	91	2	of	of	ADP
eurjchem-1125	91	3	ethyl‐2‐[({2‐[(cyanoacetyl)amino	ethyl‐2‐[({2‐[(cyanoacetyl)amino	NOUN
eurjchem-1125	91	4	]	]	PUNCT
eurjchem-1125	91	5	4,5,6,7‐	4,5,6,7‐	NUM
eurjchem-1125	91	6	tetrahydrobenzo	tetrahydrobenzo	NOUN
eurjchem-1125	91	7	[	[	X
eurjchem-1125	91	8	b]thien‐3‐yl}carbonyl)amino]‐4,5,6,7‐	b]thien‐3‐yl}carbonyl)amino]‐4,5,6,7‐	NOUN
eurjchem-1125	91	9	tetrahydro‐1‐benzothiophene‐3‐carboxylate	tetrahydro‐1‐benzothiophene‐3‐carboxylate	NOUN
eurjchem-1125	91	10	(	(	PUNCT
eurjchem-1125	91	11	7	7	NUM
eurjchem-1125	91	12	)	)	PUNCT
eurjchem-1125	91	13	with	with	ADP
eurjchem-1125	91	14	cyclic	cyclic	ADJ
eurjchem-1125	91	15	ketones	ketone	NOUN
eurjchem-1125	91	16	and	and	CCONJ
eurjchem-1125	91	17	elemental	elemental	ADJ
eurjchem-1125	91	18	sulfur	sulfur	NOUN
eurjchem-1125	91	19	general	general	ADJ
eurjchem-1125	91	20	procedure	procedure	NOUN
eurjchem-1125	91	21	:	:	PUNCT
eurjchem-1125	91	22	morpholine	morpholine	NOUN
eurjchem-1125	91	23	(	(	PUNCT
eurjchem-1125	91	24	0.33	0.33	NUM
eurjchem-1125	91	25	ml	ml	NOUN
eurjchem-1125	91	26	)	)	PUNCT
eurjchem-1125	91	27	,	,	PUNCT
eurjchem-1125	91	28	elemental	elemental	ADJ
eurjchem-1125	91	29	sulphur	sulphur	NOUN
eurjchem-1125	91	30	(	(	PUNCT
eurjchem-1125	91	31	0.141	0.141	NUM
eurjchem-1125	91	32	g	g	NOUN
eurjchem-1125	91	33	,	,	PUNCT
eurjchem-1125	91	34	4.4	4.4	NUM
eurjchem-1125	91	35	mmol	mmol	NOUN
eurjchem-1125	91	36	)	)	PUNCT
eurjchem-1125	91	37	and	and	CCONJ
eurjchem-1125	91	38	cyclohexanone	cyclohexanone	NOUN
eurjchem-1125	91	39	(	(	PUNCT
eurjchem-1125	91	40	0.4	0.4	NUM
eurjchem-1125	91	41	g	g	NOUN
eurjchem-1125	91	42	,	,	PUNCT
eurjchem-1125	91	43	4	4	NUM
eurjchem-1125	91	44	mmol	mmol	NOUN
eurjchem-1125	91	45	)	)	PUNCT
eurjchem-1125	91	46	or	or	CCONJ
eurjchem-1125	91	47	cyclopentanone	cyclopentanone	NOUN
eurjchem-1125	91	48	(	(	PUNCT
eurjchem-1125	91	49	0.34	0.34	NUM
eurjchem-1125	91	50	g	g	NOUN
eurjchem-1125	91	51	,	,	PUNCT
eurjchem-1125	91	52	4	4	NUM
eurjchem-1125	91	53	mmol	mmol	NOUN
eurjchem-1125	91	54	)	)	PUNCT
eurjchem-1125	91	55	were	be	AUX
eurjchem-1125	91	56	added	add	VERB
eurjchem-1125	91	57	to	to	ADP
eurjchem-1125	91	58	solution	solution	NOUN
eurjchem-1125	91	59	of	of	ADP
eurjchem-1125	91	60	compound	compound	NOUN
eurjchem-1125	91	61	7	7	NUM
eurjchem-1125	91	62	(	(	PUNCT
eurjchem-1125	91	63	1.88	1.88	NUM
eurjchem-1125	91	64	g	g	NOUN
eurjchem-1125	91	65	,	,	PUNCT
eurjchem-1125	91	66	4	4	NUM
eurjchem-1125	91	67	mmol	mmol	NOUN
eurjchem-1125	91	68	)	)	PUNCT
eurjchem-1125	91	69	in	in	ADP
eurjchem-1125	91	70	a	a	DET
eurjchem-1125	91	71	mixture	mixture	NOUN
eurjchem-1125	91	72	of	of	ADP
eurjchem-1125	91	73	ethanol	ethanol	NOUN
eurjchem-1125	91	74	:	:	PUNCT
eurjchem-1125	91	75	dmf	dmf	PROPN
eurjchem-1125	91	76	(	(	PUNCT
eurjchem-1125	91	77	4:1	4:1	NUM
eurjchem-1125	91	78	,	,	PUNCT
eurjchem-1125	91	79	v	v	NOUN
eurjchem-1125	91	80	:	:	PUNCT
eurjchem-1125	91	81	v	v	NOUN
eurjchem-1125	91	82	,	,	PUNCT
eurjchem-1125	91	83	25	25	NUM
eurjchem-1125	91	84	ml	ml	NOUN
eurjchem-1125	91	85	)	)	PUNCT
eurjchem-1125	91	86	.	.	PUNCT
eurjchem-1125	92	1	the	the	DET
eurjchem-1125	92	2	reaction	reaction	NOUN
eurjchem-1125	92	3	mixture	mixture	NOUN
eurjchem-1125	92	4	was	be	AUX
eurjchem-1125	92	5	heated	heat	VERB
eurjchem-1125	92	6	under	under	ADP
eurjchem-1125	92	7	reflux	reflux	NOUN
eurjchem-1125	92	8	at	at	ADP
eurjchem-1125	92	9	60‐80oc	60‐80oc	NUM
eurjchem-1125	92	10	for	for	ADP
eurjchem-1125	92	11	6	6	NUM
eurjchem-1125	92	12	h	h	NOUN
eurjchem-1125	92	13	and	and	CCONJ
eurjchem-1125	92	14	left	leave	VERB
eurjchem-1125	92	15	to	to	PART
eurjchem-1125	92	16	cool	cool	VERB
eurjchem-1125	92	17	to	to	PART
eurjchem-1125	92	18	room	room	VERB
eurjchem-1125	92	19	temperature	temperature	NOUN
eurjchem-1125	92	20	.	.	PUNCT
eurjchem-1125	93	1	the	the	DET
eurjchem-1125	93	2	separated	separate	VERB
eurjchem-1125	93	3	crystalline	crystalline	NOUN
eurjchem-1125	93	4	product	product	NOUN
eurjchem-1125	93	5	was	be	AUX
eurjchem-1125	93	6	filtered	filter	VERB
eurjchem-1125	93	7	,	,	PUNCT
eurjchem-1125	93	8	dried	dry	VERB
eurjchem-1125	93	9	,	,	PUNCT
eurjchem-1125	93	10	and	and	CCONJ
eurjchem-1125	93	11	recrystallized	recrystallize	VERB
eurjchem-1125	93	12	from	from	ADP
eurjchem-1125	93	13	dmf	dmf	PROPN
eurjchem-1125	93	14	:	:	PUNCT
eurjchem-1125	93	15	ethanol	ethanol	NOUN
eurjchem-1125	93	16	(	(	PUNCT
eurjchem-1125	93	17	2:3	2:3	NUM
eurjchem-1125	93	18	,	,	PUNCT
eurjchem-1125	93	19	v	v	NOUN
eurjchem-1125	93	20	:	:	SYM
eurjchem-1125	93	21	v	v	NOUN
eurjchem-1125	93	22	)	)	PUNCT
eurjchem-1125	93	23	to	to	PART
eurjchem-1125	93	24	give	give	VERB
eurjchem-1125	93	25	compounds	compound	NOUN
eurjchem-1125	93	26	8	8	NUM
eurjchem-1125	93	27	and	and	CCONJ
eurjchem-1125	93	28	9	9	NUM
eurjchem-1125	93	29	,	,	PUNCT
eurjchem-1125	93	30	respectively	respectively	ADV
eurjchem-1125	93	31	(	(	PUNCT
eurjchem-1125	93	32	scheme	scheme	NOUN
eurjchem-1125	93	33	2	2	NUM
eurjchem-1125	93	34	)	)	PUNCT
eurjchem-1125	93	35	.	.	PUNCT
eurjchem-1125	94	1	ethyl‐2‐{[(2‐{[(2‐amino‐5	ethyl‐2‐{[(2‐{[(2‐amino‐5	ADV
eurjchem-1125	94	2	,	,	PUNCT
eurjchem-1125	94	3	6‐dihydro‐4h‐cyclopenta[b]thien‐	6‐dihydro‐4h‐cyclopenta[b]thien‐	NUM
eurjchem-1125	94	4	3‐yl)carbonyl]amino}‐5	3‐yl)carbonyl]amino}‐5	NUM
eurjchem-1125	94	5	,	,	PUNCT
eurjchem-1125	94	6	6‐dihydro‐4h‐cyclopenta[b]‐thien‐3‐yl	6‐dihydro‐4h‐cyclopenta[b]‐thien‐3‐yl	NUM
eurjchem-1125	94	7	)	)	PUNCT
eurjchem-1125	94	8	carbonyl]amino}‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxy	carbonyl]amino}‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxy	ADJ
eurjchem-1125	95	1	late	late	ADV
eurjchem-1125	95	2	(	(	PUNCT
eurjchem-1125	95	3	8)	8)	NUM
eurjchem-1125	95	4	:	:	PUNCT
eurjchem-1125	95	5	color	color	NOUN
eurjchem-1125	95	6	:	:	PUNCT
eurjchem-1125	95	7	white	white	ADJ
eurjchem-1125	95	8	powder	powder	NOUN
eurjchem-1125	95	9	.	.	PUNCT
eurjchem-1125	96	1	yield	yield	NOUN
eurjchem-1125	96	2	:	:	PUNCT
eurjchem-1125	96	3	1.50	1.50	NUM
eurjchem-1125	96	4	g	g	NOUN
eurjchem-1125	96	5	,	,	PUNCT
eurjchem-1125	96	6	66	66	NUM
eurjchem-1125	96	7	%	%	NOUN
eurjchem-1125	96	8	.	.	PUNCT
eurjchem-1125	97	1	m.p	m.p	PROPN
eurjchem-1125	97	2	.	.	PROPN
eurjchem-1125	97	3	:	:	PUNCT
eurjchem-1125	98	1	235	235	NUM
eurjchem-1125	98	2	°	°	NUM
eurjchem-1125	98	3	c	c	X
eurjchem-1125	98	4	.	.	PUNCT
eurjchem-1125	99	1	ft‐ir	ft‐ir	NOUN
eurjchem-1125	99	2	(	(	PUNCT
eurjchem-1125	99	3	kbr	kbr	PROPN
eurjchem-1125	99	4	,	,	PUNCT
eurjchem-1125	99	5	ν	ν	PROPN
eurjchem-1125	99	6	,	,	PUNCT
eurjchem-1125	99	7	cm‐1	cm‐1	PROPN
eurjchem-1125	99	8	):	):	PUNCT
eurjchem-1125	99	9	3409	3409	NUM
eurjchem-1125	99	10	,	,	PUNCT
eurjchem-1125	99	11	3286	3286	NUM
eurjchem-1125	99	12	,	,	PUNCT
eurjchem-1125	99	13	3261	3261	NUM
eurjchem-1125	99	14	(	(	PUNCT
eurjchem-1125	99	15	nh	nh	PROPN
eurjchem-1125	99	16	,	,	PUNCT
eurjchem-1125	99	17	nh2	nh2	PROPN
eurjchem-1125	99	18	)	)	PUNCT
eurjchem-1125	99	19	,	,	PUNCT
eurjchem-1125	99	20	1668	1668	NUM
eurjchem-1125	99	21	,	,	PUNCT
eurjchem-1125	99	22	1616	1616	NUM
eurjchem-1125	99	23	(	(	PUNCT
eurjchem-1125	99	24	c	c	NOUN
eurjchem-1125	99	25	=	=	NOUN
eurjchem-1125	99	26	o	o	NOUN
eurjchem-1125	99	27	)	)	PUNCT
eurjchem-1125	99	28	.	.	PUNCT
eurjchem-1125	100	1	1h	1h	NUM
eurjchem-1125	100	2	nmr	nmr	NOUN
eurjchem-1125	100	3	(	(	PUNCT
eurjchem-1125	100	4	400	400	NUM
eurjchem-1125	100	5	mhz	mhz	NOUN
eurjchem-1125	100	6	,	,	PUNCT
eurjchem-1125	100	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	100	8	,	,	PUNCT
eurjchem-1125	100	9	δ	δ	PROPN
eurjchem-1125	100	10	,	,	PUNCT
eurjchem-1125	100	11	ppm	ppm	NUM
eurjchem-1125	100	12	):	):	PUNCT
eurjchem-1125	100	13	1.37	1.37	NUM
eurjchem-1125	100	14	(	(	PUNCT
eurjchem-1125	100	15	t	t	PROPN
eurjchem-1125	100	16	,	,	PUNCT
eurjchem-1125	100	17	3h	3h	NUM
eurjchem-1125	100	18	,	,	PUNCT
eurjchem-1125	100	19	j	j	PROPN
eurjchem-1125	100	20	=	=	SYM
eurjchem-1125	100	21	6.8	6.8	NUM
eurjchem-1125	100	22	hz	hz	NOUN
eurjchem-1125	100	23	,	,	PUNCT
eurjchem-1125	100	24	ch3	ch3	PROPN
eurjchem-1125	100	25	)	)	PUNCT
eurjchem-1125	100	26	,	,	PUNCT
eurjchem-1125	100	27	1.76‐1.85	1.76‐1.85	NUM
eurjchem-1125	100	28	(	(	PUNCT
eurjchem-1125	100	29	m	m	PROPN
eurjchem-1125	100	30	,	,	PUNCT
eurjchem-1125	100	31	8h	8h	NUM
eurjchem-1125	100	32	,	,	PUNCT
eurjchem-1125	100	33	2c5‐2h	2c5‐2h	NUM
eurjchem-1125	100	34	,	,	PUNCT
eurjchem-1125	100	35	2c6‐2h	2c6‐2h	NUM
eurjchem-1125	100	36	,	,	PUNCT
eurjchem-1125	100	37	cyclohexane	cyclohexane	NOUN
eurjchem-1125	100	38	skeleton	skeleton	NOUN
eurjchem-1125	100	39	)	)	PUNCT
eurjchem-1125	100	40	,	,	PUNCT
eurjchem-1125	100	41	2.56‐2.87	2.56‐2.87	NUM
eurjchem-1125	100	42	(	(	PUNCT
eurjchem-1125	100	43	m	m	PROPN
eurjchem-1125	100	44	,	,	PUNCT
eurjchem-1125	100	45	10h	10h	NUM
eurjchem-1125	100	46	,	,	PUNCT
eurjchem-1125	100	47	c5‐2h	c5‐2h	NOUN
eurjchem-1125	100	48	,	,	PUNCT
eurjchem-1125	100	49	cyclopentane	cyclopentane	PROPN
eurjchem-1125	100	50	skeleton	skeleton	NOUN
eurjchem-1125	100	51	,	,	PUNCT
eurjchem-1125	100	52	2c4‐2h	2c4‐2h	NUM
eurjchem-1125	100	53	,	,	PUNCT
eurjchem-1125	100	54	2c7‐2h	2c7‐2h	NUM
eurjchem-1125	100	55	,	,	PUNCT
eurjchem-1125	100	56	cyclohexane	cyclohexane	NOUN
eurjchem-1125	100	57	skeleton	skeleton	NOUN
eurjchem-1125	100	58	)	)	PUNCT
eurjchem-1125	100	59	,	,	PUNCT
eurjchem-1125	100	60	3.05‐3.35	3.05‐3.35	NUM
eurjchem-1125	100	61	(	(	PUNCT
eurjchem-1125	100	62	m	m	PROPN
eurjchem-1125	100	63	,	,	PUNCT
eurjchem-1125	100	64	4h	4h	NUM
eurjchem-1125	100	65	,	,	PUNCT
eurjchem-1125	100	66	c4‐2h	c4‐2h	PROPN
eurjchem-1125	100	67	,	,	PUNCT
eurjchem-1125	100	68	c6‐2h	c6‐2h	NOUN
eurjchem-1125	100	69	,	,	PUNCT
eurjchem-1125	100	70	cyclopentane	cyclopentane	PROPN
eurjchem-1125	100	71	skeleton	skeleton	NOUN
eurjchem-1125	100	72	)	)	PUNCT
eurjchem-1125	100	73	,	,	PUNCT
eurjchem-1125	100	74	4.33	4.33	NUM
eurjchem-1125	100	75	(	(	PUNCT
eurjchem-1125	100	76	q	q	NOUN
eurjchem-1125	100	77	,	,	PUNCT
eurjchem-1125	100	78	2h	2h	NUM
eurjchem-1125	100	79	,	,	PUNCT
eurjchem-1125	100	80	j	j	PROPN
eurjchem-1125	100	81	=	=	SYM
eurjchem-1125	100	82	6.8	6.8	NUM
eurjchem-1125	100	83	hz	hz	NOUN
eurjchem-1125	100	84	,	,	PUNCT
eurjchem-1125	100	85	ch2o	ch2o	NOUN
eurjchem-1125	100	86	)	)	PUNCT
eurjchem-1125	100	87	,	,	PUNCT
eurjchem-1125	100	88	8.20	8.20	NUM
eurjchem-1125	100	89	(	(	PUNCT
eurjchem-1125	100	90	s	s	PROPN
eurjchem-1125	100	91	,	,	PUNCT
eurjchem-1125	100	92	2h	2h	NUM
eurjchem-1125	100	93	,	,	PUNCT
eurjchem-1125	100	94	nh2	nh2	PROPN
eurjchem-1125	100	95	)	)	PUNCT
eurjchem-1125	100	96	,	,	PUNCT
eurjchem-1125	100	97	11.52	11.52	NUM
eurjchem-1125	100	98	(	(	PUNCT
eurjchem-1125	100	99	s	s	PROPN
eurjchem-1125	100	100	,	,	PUNCT
eurjchem-1125	100	101	1h	1h	NUM
eurjchem-1125	100	102	,	,	PUNCT
eurjchem-1125	100	103	nh‐co	nh‐co	NUM
eurjchem-1125	100	104	)	)	PUNCT
eurjchem-1125	100	105	,	,	PUNCT
eurjchem-1125	100	106	12.44	12.44	NUM
eurjchem-1125	100	107	(	(	PUNCT
eurjchem-1125	100	108	s	s	PROPN
eurjchem-1125	100	109	,	,	PUNCT
eurjchem-1125	100	110	1h	1h	NUM
eurjchem-1125	100	111	,	,	PUNCT
eurjchem-1125	100	112	nh‐co	nh‐co	NUM
eurjchem-1125	100	113	)	)	PUNCT
eurjchem-1125	100	114	.	.	PUNCT
eurjchem-1125	101	1	13c	13c	NOUN
eurjchem-1125	101	2	nmr	nmr	NOUN
eurjchem-1125	101	3	(	(	PUNCT
eurjchem-1125	101	4	100	100	NUM
eurjchem-1125	101	5	mhz	mhz	NOUN
eurjchem-1125	101	6	,	,	PUNCT
eurjchem-1125	101	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	101	8	,	,	PUNCT
eurjchem-1125	101	9	δ	δ	PROPN
eurjchem-1125	101	10	,	,	PUNCT
eurjchem-1125	101	11	ppm	ppm	NOUN
eurjchem-1125	101	12	):	):	PUNCT
eurjchem-1125	101	13	170.5	170.5	NUM
eurjchem-1125	101	14	,	,	PUNCT
eurjchem-1125	101	15	165.5	165.5	NUM
eurjchem-1125	101	16	,	,	PUNCT
eurjchem-1125	101	17	160.9	160.9	NUM
eurjchem-1125	101	18	,	,	PUNCT
eurjchem-1125	101	19	147.9	147.9	NUM
eurjchem-1125	101	20	,	,	PUNCT
eurjchem-1125	101	21	145.1	145.1	NUM
eurjchem-1125	101	22	,	,	PUNCT
eurjchem-1125	101	23	134.6	134.6	NUM
eurjchem-1125	101	24	,	,	PUNCT
eurjchem-1125	101	25	134.2	134.2	NUM
eurjchem-1125	101	26	,	,	PUNCT
eurjchem-1125	101	27	130.7	130.7	NUM
eurjchem-1125	101	28	,	,	PUNCT
eurjchem-1125	101	29	132.0	132.0	NUM
eurjchem-1125	101	30	,	,	PUNCT
eurjchem-1125	101	31	122.9	122.9	NUM
eurjchem-1125	101	32	,	,	PUNCT
eurjchem-1125	101	33	120.8	120.8	NUM
eurjchem-1125	101	34	,	,	PUNCT
eurjchem-1125	101	35	119.1	119.1	NUM
eurjchem-1125	101	36	,	,	PUNCT
eurjchem-1125	101	37	118.0	118.0	NUM
eurjchem-1125	101	38	,	,	PUNCT
eurjchem-1125	101	39	116.0	116.0	NUM
eurjchem-1125	101	40	,	,	PUNCT
eurjchem-1125	101	41	115.2	115.2	NUM
eurjchem-1125	101	42	,	,	PUNCT
eurjchem-1125	101	43	112.3	112.3	NUM
eurjchem-1125	101	44	,	,	PUNCT
eurjchem-1125	101	45	64.5	64.5	NUM
eurjchem-1125	101	46	,	,	PUNCT
eurjchem-1125	101	47	31.4	31.4	NUM
eurjchem-1125	101	48	,	,	PUNCT
eurjchem-1125	101	49	31.3	31.3	NUM
eurjchem-1125	101	50	,	,	PUNCT
eurjchem-1125	101	51	29.1	29.1	NUM
eurjchem-1125	101	52	,	,	PUNCT
eurjchem-1125	101	53	28.2	28.2	NUM
eurjchem-1125	101	54	,	,	PUNCT
eurjchem-1125	101	55	27.8	27.8	NUM
eurjchem-1125	101	56	,	,	PUNCT
eurjchem-1125	101	57	25.7	25.7	NUM
eurjchem-1125	101	58	,	,	PUNCT
eurjchem-1125	101	59	24.1	24.1	NUM
eurjchem-1125	101	60	,	,	PUNCT
eurjchem-1125	101	61	24.0	24.0	NUM
eurjchem-1125	101	62	,	,	PUNCT
eurjchem-1125	101	63	23.9	23.9	NUM
eurjchem-1125	101	64	,	,	PUNCT
eurjchem-1125	101	65	14.4	14.4	NUM
eurjchem-1125	101	66	.	.	PUNCT
eurjchem-1125	102	1	ei‐ms	ei‐ms	PROPN
eurjchem-1125	102	2	(	(	PUNCT
eurjchem-1125	102	3	m	m	NOUN
eurjchem-1125	102	4	/	/	SYM
eurjchem-1125	102	5	z	z	NOUN
eurjchem-1125	102	6	(	(	PUNCT
eurjchem-1125	102	7	%	%	NOUN
eurjchem-1125	102	8	)	)	PUNCT
eurjchem-1125	102	9	):	):	PUNCT
eurjchem-1125	102	10	570	570	NUM
eurjchem-1125	102	11	(	(	PUNCT
eurjchem-1125	102	12	m++1	m++1	NOUN
eurjchem-1125	102	13	,	,	PUNCT
eurjchem-1125	102	14	0.12	0.12	NUM
eurjchem-1125	102	15	)	)	PUNCT
eurjchem-1125	102	16	,	,	PUNCT
eurjchem-1125	102	17	569	569	NUM
eurjchem-1125	102	18	(	(	PUNCT
eurjchem-1125	102	19	m+	m+	NUM
eurjchem-1125	102	20	,	,	PUNCT
eurjchem-1125	102	21	0.13	0.13	NUM
eurjchem-1125	102	22	)	)	PUNCT
eurjchem-1125	102	23	,	,	PUNCT
eurjchem-1125	102	24	430	430	NUM
eurjchem-1125	102	25	(	(	PUNCT
eurjchem-1125	102	26	3.4	3.4	NUM
eurjchem-1125	102	27	)	)	PUNCT
eurjchem-1125	102	28	,	,	PUNCT
eurjchem-1125	102	29	390	390	NUM
eurjchem-1125	102	30	(	(	PUNCT
eurjchem-1125	102	31	10.7	10.7	NUM
eurjchem-1125	102	32	)	)	PUNCT
eurjchem-1125	102	33	,	,	PUNCT
eurjchem-1125	102	34	384	384	NUM
eurjchem-1125	102	35	(	(	PUNCT
eurjchem-1125	102	36	17.7	17.7	NUM
eurjchem-1125	102	37	)	)	PUNCT
eurjchem-1125	102	38	,	,	PUNCT
eurjchem-1125	102	39	370	370	NUM
eurjchem-1125	102	40	(	(	PUNCT
eurjchem-1125	102	41	14.9	14.9	NUM
eurjchem-1125	102	42	)	)	PUNCT
eurjchem-1125	102	43	,	,	PUNCT
eurjchem-1125	102	44	344	344	NUM
eurjchem-1125	102	45	(	(	PUNCT
eurjchem-1125	102	46	6.42	6.42	NUM
eurjchem-1125	102	47	)	)	PUNCT
eurjchem-1125	102	48	,	,	PUNCT
eurjchem-1125	102	49	225	225	NUM
eurjchem-1125	102	50	(	(	PUNCT
eurjchem-1125	102	51	73.5	73.5	NUM
eurjchem-1125	102	52	)	)	PUNCT
eurjchem-1125	102	53	,	,	PUNCT
eurjchem-1125	102	54	205	205	NUM
eurjchem-1125	102	55	(	(	PUNCT
eurjchem-1125	102	56	26.8	26.8	NUM
eurjchem-1125	102	57	)	)	PUNCT
eurjchem-1125	102	58	,	,	PUNCT
eurjchem-1125	102	59	178	178	NUM
eurjchem-1125	102	60	(	(	PUNCT
eurjchem-1125	102	61	100	100	NUM
eurjchem-1125	102	62	)	)	PUNCT
eurjchem-1125	102	63	,	,	PUNCT
eurjchem-1125	102	64	165	165	NUM
eurjchem-1125	102	65	(	(	PUNCT
eurjchem-1125	102	66	76.5	76.5	NUM
eurjchem-1125	102	67	)	)	PUNCT
eurjchem-1125	102	68	,	,	PUNCT
eurjchem-1125	102	69	150	150	NUM
eurjchem-1125	102	70	(	(	PUNCT
eurjchem-1125	102	71	64.3	64.3	NUM
eurjchem-1125	102	72	)	)	PUNCT
eurjchem-1125	102	73	,	,	PUNCT
eurjchem-1125	102	74	138	138	NUM
eurjchem-1125	102	75	(	(	PUNCT
eurjchem-1125	102	76	25.1	25.1	NUM
eurjchem-1125	102	77	)	)	PUNCT
eurjchem-1125	102	78	,	,	PUNCT
eurjchem-1125	102	79	122	122	NUM
eurjchem-1125	102	80	(	(	PUNCT
eurjchem-1125	102	81	38.1	38.1	NUM
eurjchem-1125	102	82	)	)	PUNCT
eurjchem-1125	102	83	,	,	PUNCT
eurjchem-1125	102	84	109	109	NUM
eurjchem-1125	102	85	(	(	PUNCT
eurjchem-1125	102	86	29.2	29.2	NUM
eurjchem-1125	102	87	)	)	PUNCT
eurjchem-1125	102	88	,	,	PUNCT
eurjchem-1125	102	89	103	103	NUM
eurjchem-1125	102	90	(	(	PUNCT
eurjchem-1125	102	91	27.2	27.2	NUM
eurjchem-1125	102	92	)	)	PUNCT
eurjchem-1125	102	93	,	,	PUNCT
eurjchem-1125	102	94	90	90	NUM
eurjchem-1125	102	95	(	(	PUNCT
eurjchem-1125	102	96	25.5	25.5	NUM
eurjchem-1125	102	97	)	)	PUNCT
eurjchem-1125	102	98	,	,	PUNCT
eurjchem-1125	102	99	77	77	NUM
eurjchem-1125	102	100	(	(	PUNCT
eurjchem-1125	102	101	34.1	34.1	NUM
eurjchem-1125	102	102	)	)	PUNCT
eurjchem-1125	102	103	,	,	PUNCT
eurjchem-1125	102	104	64	64	NUM
eurjchem-1125	102	105	(	(	PUNCT
eurjchem-1125	102	106	27.5	27.5	NUM
eurjchem-1125	102	107	)	)	PUNCT
eurjchem-1125	102	108	.	.	PUNCT
eurjchem-1125	103	1	anal	anal	PROPN
eurjchem-1125	103	2	.	.	PUNCT
eurjchem-1125	103	3	calcd	calcd	NOUN
eurjchem-1125	103	4	.	.	PUNCT
eurjchem-1125	104	1	for	for	ADP
eurjchem-1125	104	2	c28h31n3o4s3	c28h31n3o4s3	NOUN
eurjchem-1125	104	3	:	:	PUNCT
eurjchem-1125	104	4	c	c	X
eurjchem-1125	104	5	,	,	PUNCT
eurjchem-1125	104	6	59.02	59.02	NUM
eurjchem-1125	104	7	;	;	PUNCT
eurjchem-1125	104	8	h	h	X
eurjchem-1125	104	9	,	,	PUNCT
eurjchem-1125	104	10	5.48	5.48	NUM
eurjchem-1125	104	11	;	;	PUNCT
eurjchem-1125	104	12	n	n	CCONJ
eurjchem-1125	104	13	,	,	PUNCT
eurjchem-1125	104	14	7.38	7.38	NUM
eurjchem-1125	104	15	.	.	PUNCT
eurjchem-1125	104	16	found	find	VERB
eurjchem-1125	104	17	:	:	PUNCT
eurjchem-1125	105	1	c	c	X
eurjchem-1125	105	2	,	,	PUNCT
eurjchem-1125	105	3	58.98	58.98	NUM
eurjchem-1125	105	4	;	;	PUNCT
eurjchem-1125	105	5	h	h	NOUN
eurjchem-1125	105	6	,	,	PUNCT
eurjchem-1125	105	7	5.45	5.45	NUM
eurjchem-1125	105	8	;	;	PUNCT
eurjchem-1125	105	9	n	n	CCONJ
eurjchem-1125	105	10	,	,	PUNCT
eurjchem-1125	105	11	7.40	7.40	NUM
eurjchem-1125	105	12	%	%	NOUN
eurjchem-1125	105	13	.	.	PUNCT
eurjchem-1125	106	1	ethyl‐2‐{[(2‐{[(2‐amino‐4	ethyl‐2‐{[(2‐{[(2‐amino‐4	PROPN
eurjchem-1125	106	2	,	,	PUNCT
eurjchem-1125	106	3	5	5	NUM
eurjchem-1125	106	4	,	,	PUNCT
eurjchem-1125	106	5	6	6	NUM
eurjchem-1125	106	6	,	,	PUNCT
eurjchem-1125	106	7	7‐tetrahydro‐1‐benzothien‐3‐	7‐tetrahydro‐1‐benzothien‐3‐	PROPN
eurjchem-1125	106	8	yl)carbonyl]amino}‐4,5,6	yl)carbonyl]amino}‐4,5,6	NOUN
eurjchem-1125	106	9	,	,	PUNCT
eurjchem-1125	106	10	7‐tetrahydro‐1‐benzothien‐3‐yl)carbon	7‐tetrahydro‐1‐benzothien‐3‐yl)carbon	PRON
eurjchem-1125	106	11	yl]amino}‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxylate	yl]amino}‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxylate	NOUN
eurjchem-1125	106	12	(	(	PUNCT
eurjchem-1125	106	13	9	9	NUM
eurjchem-1125	106	14	):	):	PUNCT
eurjchem-1125	106	15	color	color	NOUN
eurjchem-1125	106	16	:	:	PUNCT
eurjchem-1125	106	17	white	white	ADJ
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eurjchem-1125	106	19	.	.	PUNCT
eurjchem-1125	107	1	yield	yield	NOUN
eurjchem-1125	107	2	:	:	PUNCT
eurjchem-1125	107	3	1.61	1.61	NUM
eurjchem-1125	107	4	g	g	NOUN
eurjchem-1125	107	5	,	,	PUNCT
eurjchem-1125	107	6	69	69	NUM
eurjchem-1125	107	7	%	%	NOUN
eurjchem-1125	107	8	.	.	PUNCT
eurjchem-1125	108	1	m.p	m.p	PROPN
eurjchem-1125	108	2	.	.	PROPN
eurjchem-1125	108	3	:	:	PUNCT
eurjchem-1125	109	1	255	255	NUM
eurjchem-1125	109	2	°	°	NUM
eurjchem-1125	109	3	c	c	X
eurjchem-1125	109	4	.	.	PUNCT
eurjchem-1125	110	1	ft‐ir	ft‐ir	NOUN
eurjchem-1125	110	2	(	(	PUNCT
eurjchem-1125	110	3	kbr	kbr	PROPN
eurjchem-1125	110	4	,	,	PUNCT
eurjchem-1125	110	5	ν	ν	PROPN
eurjchem-1125	110	6	,	,	PUNCT
eurjchem-1125	110	7	cm‐1	cm‐1	PROPN
eurjchem-1125	110	8	):	):	PUNCT
eurjchem-1125	110	9	3419	3419	NUM
eurjchem-1125	110	10	,	,	PUNCT
eurjchem-1125	110	11	3282	3282	NUM
eurjchem-1125	110	12	,	,	PUNCT
eurjchem-1125	110	13	3265	3265	NUM
eurjchem-1125	110	14	(	(	PUNCT
eurjchem-1125	110	15	nh	nh	NOUN
eurjchem-1125	110	16	,	,	PUNCT
eurjchem-1125	110	17	nh2	nh2	PROPN
eurjchem-1125	110	18	)	)	PUNCT
eurjchem-1125	110	19	,	,	PUNCT
eurjchem-1125	110	20	1660	1660	NUM
eurjchem-1125	110	21	,	,	PUNCT
eurjchem-1125	110	22	1610	1610	NUM
eurjchem-1125	110	23	(	(	PUNCT
eurjchem-1125	110	24	c	c	NOUN
eurjchem-1125	110	25	=	=	NOUN
eurjchem-1125	110	26	o	o	NOUN
eurjchem-1125	110	27	)	)	PUNCT
eurjchem-1125	110	28	.	.	PUNCT
eurjchem-1125	111	1	1h	1h	NUM
eurjchem-1125	111	2	nmr	nmr	NOUN
eurjchem-1125	111	3	(	(	PUNCT
eurjchem-1125	111	4	400	400	NUM
eurjchem-1125	111	5	mhz	mhz	NOUN
eurjchem-1125	111	6	,	,	PUNCT
eurjchem-1125	111	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	111	8	,	,	PUNCT
eurjchem-1125	111	9	δ	δ	PROPN
eurjchem-1125	111	10	,	,	PUNCT
eurjchem-1125	111	11	ppm	ppm	NUM
eurjchem-1125	111	12	):	):	PUNCT
eurjchem-1125	111	13	1.35	1.35	NUM
eurjchem-1125	111	14	(	(	PUNCT
eurjchem-1125	111	15	t	t	PROPN
eurjchem-1125	111	16	,	,	PUNCT
eurjchem-1125	111	17	3h	3h	NUM
eurjchem-1125	111	18	,	,	PUNCT
eurjchem-1125	111	19	j	j	PROPN
eurjchem-1125	111	20	=	=	SYM
eurjchem-1125	111	21	6.8	6.8	NUM
eurjchem-1125	111	22	hz	hz	NOUN
eurjchem-1125	111	23	,	,	PUNCT
eurjchem-1125	111	24	ch3	ch3	PROPN
eurjchem-1125	111	25	)	)	PUNCT
eurjchem-1125	111	26	,	,	PUNCT
eurjchem-1125	111	27	1.71‐1.82	1.71‐1.82	NUM
eurjchem-1125	111	28	(	(	PUNCT
eurjchem-1125	111	29	m	m	PROPN
eurjchem-1125	111	30	,	,	PUNCT
eurjchem-1125	111	31	12h	12h	NUM
eurjchem-1125	111	32	,	,	PUNCT
eurjchem-1125	111	33	3c5‐2h	3c5‐2h	NUM
eurjchem-1125	111	34	,	,	PUNCT
eurjchem-1125	111	35	3c6‐2h	3c6‐2h	NUM
eurjchem-1125	111	36	,	,	PUNCT
eurjchem-1125	111	37	cyclohexane	cyclohexane	NOUN
eurjchem-1125	111	38	skeleton	skeleton	NOUN
eurjchem-1125	111	39	)	)	PUNCT
eurjchem-1125	111	40	,	,	PUNCT
eurjchem-1125	111	41	2.77‐2.87	2.77‐2.87	PROPN
eurjchem-1125	111	42	(	(	PUNCT
eurjchem-1125	111	43	m	m	PROPN
eurjchem-1125	111	44	,	,	PUNCT
eurjchem-1125	111	45	12h	12h	NUM
eurjchem-1125	111	46	,	,	PUNCT
eurjchem-1125	111	47	3c4‐2h	3c4‐2h	NUM
eurjchem-1125	111	48	,	,	PUNCT
eurjchem-1125	111	49	3c7‐2h	3c7‐2h	NUM
eurjchem-1125	111	50	,	,	PUNCT
eurjchem-1125	111	51	cyclohexane	cyclohexane	NOUN
eurjchem-1125	111	52	skeleton	skeleton	NOUN
eurjchem-1125	111	53	)	)	PUNCT
eurjchem-1125	111	54	,	,	PUNCT
eurjchem-1125	111	55	4.33	4.33	NUM
eurjchem-1125	111	56	(	(	PUNCT
eurjchem-1125	111	57	q	q	NOUN
eurjchem-1125	111	58	,	,	PUNCT
eurjchem-1125	111	59	2h	2h	NUM
eurjchem-1125	111	60	,	,	PUNCT
eurjchem-1125	111	61	j	j	PROPN
eurjchem-1125	111	62	=	=	SYM
eurjchem-1125	111	63	6.8	6.8	NUM
eurjchem-1125	111	64	hz	hz	NOUN
eurjchem-1125	111	65	,	,	PUNCT
eurjchem-1125	111	66	ch2o	ch2o	NOUN
eurjchem-1125	111	67	)	)	PUNCT
eurjchem-1125	111	68	,	,	PUNCT
eurjchem-1125	111	69	8.20	8.20	NUM
eurjchem-1125	111	70	(	(	PUNCT
eurjchem-1125	111	71	s	s	PROPN
eurjchem-1125	111	72	,	,	PUNCT
eurjchem-1125	111	73	2h	2h	NUM
eurjchem-1125	111	74	,	,	PUNCT
eurjchem-1125	111	75	nh2	nh2	PROPN
eurjchem-1125	111	76	)	)	PUNCT
eurjchem-1125	111	77	,	,	PUNCT
eurjchem-1125	111	78	11.62	11.62	NUM
eurjchem-1125	111	79	(	(	PUNCT
eurjchem-1125	111	80	s	s	PROPN
eurjchem-1125	111	81	,	,	PUNCT
eurjchem-1125	111	82	1h	1h	NUM
eurjchem-1125	111	83	,	,	PUNCT
eurjchem-1125	111	84	nh‐co	nh‐co	NUM
eurjchem-1125	111	85	)	)	PUNCT
eurjchem-1125	111	86	,	,	PUNCT
eurjchem-1125	111	87	11.80	11.80	NUM
eurjchem-1125	111	88	(	(	PUNCT
eurjchem-1125	111	89	s	s	PROPN
eurjchem-1125	111	90	,	,	PUNCT
eurjchem-1125	111	91	1h	1h	NUM
eurjchem-1125	111	92	,	,	PUNCT
eurjchem-1125	111	93	nh‐co	nh‐co	NUM
eurjchem-1125	111	94	)	)	PUNCT
eurjchem-1125	111	95	.	.	PUNCT
eurjchem-1125	112	1	ei‐ms	ei‐ms	PROPN
eurjchem-1125	112	2	(	(	PUNCT
eurjchem-1125	112	3	m	m	NOUN
eurjchem-1125	112	4	/	/	SYM
eurjchem-1125	112	5	z	z	NOUN
eurjchem-1125	112	6	(	(	PUNCT
eurjchem-1125	112	7	%	%	NOUN
eurjchem-1125	112	8	)	)	PUNCT
eurjchem-1125	112	9	):	):	PUNCT
eurjchem-1125	112	10	584	584	NUM
eurjchem-1125	112	11	(	(	PUNCT
eurjchem-1125	112	12	m++1	m++1	NOUN
eurjchem-1125	112	13	,	,	PUNCT
eurjchem-1125	112	14	0.2	0.2	NUM
eurjchem-1125	112	15	)	)	PUNCT
eurjchem-1125	112	16	,	,	PUNCT
eurjchem-1125	112	17	483	483	NUM
eurjchem-1125	112	18	(	(	PUNCT
eurjchem-1125	112	19	0.2	0.2	NUM
eurjchem-1125	112	20	,	,	PUNCT
eurjchem-1125	112	21	m+	m+	NUM
eurjchem-1125	112	22	)	)	PUNCT
eurjchem-1125	112	23	,	,	PUNCT
eurjchem-1125	112	24	465	465	NUM
eurjchem-1125	112	25	(	(	PUNCT
eurjchem-1125	112	26	0.3	0.3	NUM
eurjchem-1125	112	27	)	)	PUNCT
eurjchem-1125	112	28	,	,	PUNCT
eurjchem-1125	112	29	405	405	NUM
eurjchem-1125	112	30	(	(	PUNCT
eurjchem-1125	112	31	0.9	0.9	NUM
eurjchem-1125	112	32	)	)	PUNCT
eurjchem-1125	112	33	,	,	PUNCT
eurjchem-1125	112	34	385	385	NUM
eurjchem-1125	112	35	(	(	PUNCT
eurjchem-1125	112	36	0.4	0.4	NUM
eurjchem-1125	112	37	)	)	PUNCT
eurjchem-1125	112	38	,	,	PUNCT
eurjchem-1125	112	39	357	357	NUM
eurjchem-1125	112	40	(	(	PUNCT
eurjchem-1125	112	41	0.2	0.2	NUM
eurjchem-1125	112	42	)	)	PUNCT
eurjchem-1125	112	43	,	,	PUNCT
eurjchem-1125	112	44	314	314	NUM
eurjchem-1125	112	45	(	(	PUNCT
eurjchem-1125	112	46	0.3	0.3	NUM
eurjchem-1125	112	47	)	)	PUNCT
eurjchem-1125	112	48	,	,	PUNCT
eurjchem-1125	112	49	258	258	NUM
eurjchem-1125	112	50	(	(	PUNCT
eurjchem-1125	112	51	1.7	1.7	NUM
eurjchem-1125	112	52	)	)	PUNCT
eurjchem-1125	112	53	,	,	PUNCT
eurjchem-1125	112	54	224	224	NUM
eurjchem-1125	112	55	(	(	PUNCT
eurjchem-1125	112	56	8.4	8.4	NUM
eurjchem-1125	112	57	)	)	PUNCT
eurjchem-1125	112	58	,	,	PUNCT
eurjchem-1125	112	59	179	179	NUM
eurjchem-1125	112	60	(	(	PUNCT
eurjchem-1125	112	61	100	100	NUM
eurjchem-1125	112	62	)	)	PUNCT
eurjchem-1125	112	63	,	,	PUNCT
eurjchem-1125	112	64	150	150	NUM
eurjchem-1125	112	65	(	(	PUNCT
eurjchem-1125	112	66	67.0	67.0	NUM
eurjchem-1125	112	67	)	)	PUNCT
eurjchem-1125	112	68	,	,	PUNCT
eurjchem-1125	112	69	123	123	NUM
eurjchem-1125	112	70	(	(	PUNCT
eurjchem-1125	112	71	61.2	61.2	NUM
eurjchem-1125	112	72	)	)	PUNCT
eurjchem-1125	112	73	,	,	PUNCT
eurjchem-1125	112	74	128	128	NUM
eurjchem-1125	112	75	(	(	PUNCT
eurjchem-1125	112	76	2.1	2.1	NUM
eurjchem-1125	112	77	)	)	PUNCT
eurjchem-1125	112	78	,	,	PUNCT
eurjchem-1125	112	79	117	117	NUM
eurjchem-1125	112	80	(	(	PUNCT
eurjchem-1125	112	81	39.1	39.1	NUM
eurjchem-1125	112	82	)	)	PUNCT
eurjchem-1125	112	83	,	,	PUNCT
eurjchem-1125	112	84	91	91	NUM
eurjchem-1125	112	85	(	(	PUNCT
eurjchem-1125	112	86	29.6	29.6	NUM
eurjchem-1125	112	87	)	)	PUNCT
eurjchem-1125	112	88	,	,	PUNCT
eurjchem-1125	112	89	76	76	NUM
eurjchem-1125	112	90	(	(	PUNCT
eurjchem-1125	112	91	41.2	41.2	NUM
eurjchem-1125	112	92	)	)	PUNCT
eurjchem-1125	112	93	,	,	PUNCT
eurjchem-1125	112	94	50	50	NUM
eurjchem-1125	112	95	(	(	PUNCT
eurjchem-1125	112	96	38.1	38.1	NUM
eurjchem-1125	112	97	)	)	PUNCT
eurjchem-1125	112	98	.	.	PUNCT
eurjchem-1125	113	1	anal	anal	PROPN
eurjchem-1125	113	2	.	.	PUNCT
eurjchem-1125	113	3	calcd	calcd	NOUN
eurjchem-1125	113	4	.	.	PUNCT
eurjchem-1125	114	1	for	for	ADP
eurjchem-1125	114	2	c29h33n3o4s3	c29h33n3o4s3	NOUN
eurjchem-1125	114	3	:	:	PUNCT
eurjchem-1125	114	4	c	c	X
eurjchem-1125	114	5	,	,	PUNCT
eurjchem-1125	114	6	59.66	59.66	NUM
eurjchem-1125	114	7	;	;	PUNCT
eurjchem-1125	114	8	h	h	NOUN
eurjchem-1125	114	9	,	,	PUNCT
eurjchem-1125	114	10	5.70	5.70	NUM
eurjchem-1125	114	11	;	;	PUNCT
eurjchem-1125	114	12	n	n	CCONJ
eurjchem-1125	114	13	,	,	PUNCT
eurjchem-1125	114	14	7.20	7.20	NUM
eurjchem-1125	114	15	.	.	PUNCT
eurjchem-1125	114	16	found	find	VERB
eurjchem-1125	114	17	:	:	PUNCT
eurjchem-1125	115	1	c	c	X
eurjchem-1125	115	2	,	,	PUNCT
eurjchem-1125	115	3	59.61	59.61	NUM
eurjchem-1125	115	4	;	;	PUNCT
eurjchem-1125	115	5	h	h	X
eurjchem-1125	115	6	,	,	PUNCT
eurjchem-1125	115	7	5.72	5.72	NUM
eurjchem-1125	115	8	;	;	PUNCT
eurjchem-1125	115	9	n	n	CCONJ
eurjchem-1125	115	10	,	,	PUNCT
eurjchem-1125	115	11	7.18	7.18	NUM
eurjchem-1125	115	12	%	%	NOUN
eurjchem-1125	115	13	.	.	PUNCT
eurjchem-1125	116	1	2.2.4	2.2.4	X
eurjchem-1125	116	2	.	.	PUNCT
eurjchem-1125	116	3	reaction	reaction	NOUN
eurjchem-1125	116	4	of	of	ADP
eurjchem-1125	116	5	ethyl‐2‐[({2‐[(cyanoacetyl)amino]‐4,5,6,7‐	ethyl‐2‐[({2‐[(cyanoacetyl)amino]‐4,5,6,7‐	PROPN
eurjchem-1125	116	6	tetrahydrobenzo[b]thien‐3‐yl}carbonyl)amino]‐4,5,6,7‐tetra	tetrahydrobenzo[b]thien‐3‐yl}carbonyl)amino]‐4,5,6,7‐tetra	PUNCT
eurjchem-1125	116	7	hydro‐1‐benzothiophene‐3‐carboxylate	hydro‐1‐benzothiophene‐3‐carboxylate	PROPN
eurjchem-1125	116	8	(	(	PUNCT
eurjchem-1125	116	9	7	7	NUM
eurjchem-1125	116	10	)	)	PUNCT
eurjchem-1125	116	11	with	with	ADP
eurjchem-1125	116	12	aromatic	aromatic	ADJ
eurjchem-1125	116	13	aldehydes	aldehyde	NOUN
eurjchem-1125	116	14	general	general	ADJ
eurjchem-1125	116	15	procedure	procedure	NOUN
eurjchem-1125	116	16	:	:	PUNCT
eurjchem-1125	116	17	a	a	DET
eurjchem-1125	116	18	mixture	mixture	NOUN
eurjchem-1125	116	19	of	of	ADP
eurjchem-1125	116	20	compound	compound	NOUN
eurjchem-1125	116	21	7	7	NUM
eurjchem-1125	116	22	(	(	PUNCT
eurjchem-1125	116	23	1.17	1.17	NUM
eurjchem-1125	116	24	g	g	NOUN
eurjchem-1125	116	25	,	,	PUNCT
eurjchem-1125	116	26	2.5	2.5	NUM
eurjchem-1125	116	27	mmol	mmol	NOUN
eurjchem-1125	116	28	)	)	PUNCT
eurjchem-1125	116	29	,	,	PUNCT
eurjchem-1125	116	30	4‐(dimethylamino	4‐(dimethylamino	ADJ
eurjchem-1125	116	31	)	)	PUNCT
eurjchem-1125	116	32	benzaldehyde	benzaldehyde	NOUN
eurjchem-1125	116	33	(	(	PUNCT
eurjchem-1125	116	34	0.37	0.37	NUM
eurjchem-1125	116	35	g	g	NOUN
eurjchem-1125	116	36	,	,	PUNCT
eurjchem-1125	116	37	2.5	2.5	NUM
eurjchem-1125	116	38	mmol	mmol	NOUN
eurjchem-1125	116	39	)	)	PUNCT
eurjchem-1125	116	40	,	,	PUNCT
eurjchem-1125	116	41	4‐	4‐	NUM
eurjchem-1125	116	42	(	(	PUNCT
eurjchem-1125	116	43	piperidin‐1‐yl)benzaldehyde	piperidin‐1‐yl)benzaldehyde	PROPN
eurjchem-1125	116	44	(	(	PUNCT
eurjchem-1125	116	45	0.47	0.47	NUM
eurjchem-1125	116	46	g	g	NOUN
eurjchem-1125	116	47	,	,	PUNCT
eurjchem-1125	116	48	2.5	2.5	NUM
eurjchem-1125	116	49	mmol	mmol	NOUN
eurjchem-1125	116	50	)	)	PUNCT
eurjchem-1125	116	51	,	,	PUNCT
eurjchem-1125	116	52	or	or	CCONJ
eurjchem-1125	116	53	2‐hydroxy	2‐hydroxy	NUM
eurjchem-1125	116	54	benzaldehyde	benzaldehyde	NOUN
eurjchem-1125	116	55	(	(	PUNCT
eurjchem-1125	116	56	0.31	0.31	NUM
eurjchem-1125	116	57	g	g	NOUN
eurjchem-1125	116	58	,	,	PUNCT
eurjchem-1125	116	59	2.5	2.5	NUM
eurjchem-1125	116	60	mmol	mmol	NOUN
eurjchem-1125	116	61	)	)	PUNCT
eurjchem-1125	116	62	in	in	ADP
eurjchem-1125	116	63	ethanol	ethanol	NOUN
eurjchem-1125	116	64	(	(	PUNCT
eurjchem-1125	116	65	15	15	NUM
eurjchem-1125	116	66	ml	ml	NOUN
eurjchem-1125	116	67	)	)	PUNCT
eurjchem-1125	116	68	containing	contain	VERB
eurjchem-1125	116	69	piperidine	piperidine	NOUN
eurjchem-1125	116	70	(	(	PUNCT
eurjchem-1125	116	71	0.2	0.2	NUM
eurjchem-1125	116	72	ml	ml	NOUN
eurjchem-1125	116	73	)	)	PUNCT
eurjchem-1125	116	74	was	be	AUX
eurjchem-1125	116	75	stirred	stir	VERB
eurjchem-1125	116	76	at	at	ADP
eurjchem-1125	116	77	80	80	NUM
eurjchem-1125	116	78	°	°	NUM
eurjchem-1125	116	79	c	c	NOUN
eurjchem-1125	116	80	for	for	ADP
eurjchem-1125	116	81	4	4	NUM
eurjchem-1125	116	82	h.	h.	NOUN
eurjchem-1125	116	83	the	the	DET
eurjchem-1125	116	84	separated	separate	VERB
eurjchem-1125	116	85	crystals	crystal	NOUN
eurjchem-1125	116	86	was	be	AUX
eurjchem-1125	116	87	filtered	filter	VERB
eurjchem-1125	116	88	,	,	PUNCT
eurjchem-1125	116	89	dried	dry	VERB
eurjchem-1125	116	90	and	and	CCONJ
eurjchem-1125	116	91	washed	wash	VERB
eurjchem-1125	116	92	with	with	ADP
eurjchem-1125	116	93	hot	hot	PROPN
eurjchem-1125	116	94	dmf	dmf	PROPN
eurjchem-1125	116	95	to	to	PART
eurjchem-1125	116	96	give	give	VERB
eurjchem-1125	116	97	compounds	compound	NOUN
eurjchem-1125	116	98	10‐12	10‐12	NUM
eurjchem-1125	116	99	,	,	PUNCT
eurjchem-1125	116	100	respectively	respectively	ADV
eurjchem-1125	116	101	(	(	PUNCT
eurjchem-1125	116	102	scheme	scheme	NOUN
eurjchem-1125	116	103	2	2	NUM
eurjchem-1125	116	104	)	)	PUNCT
eurjchem-1125	116	105	.	.	PUNCT
eurjchem-1125	117	1	ethyl	ethyl	PROPN
eurjchem-1125	117	2	2‐({[2‐({(2e)‐2‐cyano‐3‐[4‐(dimethylamino)phenyl	2‐({[2‐({(2e)‐2‐cyano‐3‐[4‐(dimethylamino)phenyl	NUM
eurjchem-1125	117	3	]	]	X
eurjchem-1125	118	1	prop‐2‐enoyl}amino)‐4	prop‐2‐enoyl}amino)‐4	ADJ
eurjchem-1125	118	2	,	,	PUNCT
eurjchem-1125	118	3	5	5	NUM
eurjchem-1125	118	4	,	,	PUNCT
eurjchem-1125	118	5	6	6	NUM
eurjchem-1125	118	6	,	,	PUNCT
eurjchem-1125	118	7	7‐tetrahydro‐1‐benzothien‐3‐yl	7‐tetrahydro‐1‐benzothien‐3‐yl	NUM
eurjchem-1125	118	8	]	]	PUNCT
eurjchem-1125	118	9	carbonyl}amino)‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxy	carbonyl}amino)‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxy	PROPN
eurjchem-1125	118	10	late	late	ADJ
eurjchem-1125	118	11	(	(	PUNCT
eurjchem-1125	118	12	10	10	NUM
eurjchem-1125	118	13	):	):	PUNCT
eurjchem-1125	118	14	color	color	NOUN
eurjchem-1125	118	15	:	:	PUNCT
eurjchem-1125	118	16	red	red	ADJ
eurjchem-1125	118	17	needle	needle	NOUN
eurjchem-1125	118	18	crystals	crystal	NOUN
eurjchem-1125	118	19	.	.	PUNCT
eurjchem-1125	119	1	yield	yield	NOUN
eurjchem-1125	119	2	:	:	PUNCT
eurjchem-1125	119	3	1.43	1.43	NUM
eurjchem-1125	119	4	g	g	NOUN
eurjchem-1125	119	5	,	,	PUNCT
eurjchem-1125	119	6	95	95	NUM
eurjchem-1125	119	7	%	%	NOUN
eurjchem-1125	119	8	.	.	PUNCT
eurjchem-1125	120	1	m.p	m.p	PROPN
eurjchem-1125	120	2	.	.	PROPN
eurjchem-1125	120	3	:	:	PUNCT
eurjchem-1125	121	1	>	>	X
eurjchem-1125	121	2	320	320	NUM
eurjchem-1125	121	3	°	°	NOUN
eurjchem-1125	121	4	c	c	NOUN
eurjchem-1125	121	5	.	.	PUNCT
eurjchem-1125	122	1	ft‐ir	ft‐ir	NOUN
eurjchem-1125	122	2	(	(	PUNCT
eurjchem-1125	122	3	kbr	kbr	PROPN
eurjchem-1125	122	4	,	,	PUNCT
eurjchem-1125	122	5	ν	ν	PROPN
eurjchem-1125	122	6	,	,	PUNCT
eurjchem-1125	122	7	cm‐1	cm‐1	PROPN
eurjchem-1125	122	8	):	):	PUNCT
eurjchem-1125	122	9	3293	3293	NUM
eurjchem-1125	122	10	,	,	PUNCT
eurjchem-1125	122	11	3183	3183	NUM
eurjchem-1125	122	12	(	(	PUNCT
eurjchem-1125	122	13	2nh	2nh	NOUN
eurjchem-1125	122	14	)	)	PUNCT
eurjchem-1125	122	15	,	,	PUNCT
eurjchem-1125	122	16	2196	2196	NUM
eurjchem-1125	122	17	(	(	PUNCT
eurjchem-1125	122	18	cn	cn	NOUN
eurjchem-1125	122	19	)	)	PUNCT
eurjchem-1125	122	20	,	,	PUNCT
eurjchem-1125	122	21	1688	1688	NUM
eurjchem-1125	122	22	,	,	PUNCT
eurjchem-1125	122	23	1614	1614	NUM
eurjchem-1125	122	24	(	(	PUNCT
eurjchem-1125	122	25	c	c	NOUN
eurjchem-1125	122	26	=	=	NOUN
eurjchem-1125	122	27	o	o	NOUN
eurjchem-1125	122	28	)	)	PUNCT
eurjchem-1125	122	29	.	.	PUNCT
eurjchem-1125	123	1	ei‐ms	ei‐ms	PROPN
eurjchem-1125	123	2	(	(	PUNCT
eurjchem-1125	123	3	m	m	NOUN
eurjchem-1125	123	4	/	/	SYM
eurjchem-1125	123	5	z	z	NOUN
eurjchem-1125	123	6	(	(	PUNCT
eurjchem-1125	123	7	%	%	NOUN
eurjchem-1125	123	8	)	)	PUNCT
eurjchem-1125	123	9	):	):	PUNCT
eurjchem-1125	123	10	605	605	NUM
eurjchem-1125	123	11	(	(	PUNCT
eurjchem-1125	123	12	m++3	m++3	NOUN
eurjchem-1125	123	13	,	,	PUNCT
eurjchem-1125	123	14	29.4	29.4	NUM
eurjchem-1125	123	15	)	)	PUNCT
eurjchem-1125	123	16	,	,	PUNCT
eurjchem-1125	123	17	604	604	NUM
eurjchem-1125	123	18	(	(	PUNCT
eurjchem-1125	123	19	m++2	m++2	PROPN
eurjchem-1125	123	20	,	,	PUNCT
eurjchem-1125	123	21	35.3	35.3	NUM
eurjchem-1125	123	22	)	)	PUNCT
eurjchem-1125	123	23	,	,	PUNCT
eurjchem-1125	123	24	255	255	NUM
eurjchem-1125	123	25	(	(	PUNCT
eurjchem-1125	123	26	100	100	NUM
eurjchem-1125	123	27	)	)	PUNCT
eurjchem-1125	123	28	,	,	PUNCT
eurjchem-1125	123	29	180	180	NUM
eurjchem-1125	123	30	(	(	PUNCT
eurjchem-1125	123	31	70.6	70.6	NUM
eurjchem-1125	123	32	)	)	PUNCT
eurjchem-1125	123	33	,	,	PUNCT
eurjchem-1125	123	34	179	179	NUM
eurjchem-1125	123	35	(	(	PUNCT
eurjchem-1125	123	36	76.5	76.5	NUM
eurjchem-1125	123	37	)	)	PUNCT
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eurjchem-1125	123	42	)	)	PUNCT
eurjchem-1125	123	43	,	,	PUNCT
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eurjchem-1125	123	45	(	(	PUNCT
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eurjchem-1125	123	57	)	)	PUNCT
eurjchem-1125	123	58	.	.	PUNCT
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eurjchem-1125	124	4	.	.	PUNCT
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eurjchem-1125	125	5	,	,	PUNCT
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eurjchem-1125	125	7	;	;	PUNCT
eurjchem-1125	126	1	h	h	NOUN
eurjchem-1125	126	2	,	,	PUNCT
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eurjchem-1125	126	4	;	;	PUNCT
eurjchem-1125	126	5	n	n	CCONJ
eurjchem-1125	126	6	,	,	PUNCT
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eurjchem-1125	127	2	,	,	PUNCT
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eurjchem-1125	127	4	;	;	PUNCT
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eurjchem-1125	127	6	,	,	PUNCT
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eurjchem-1125	127	8	;	;	PUNCT
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eurjchem-1125	127	10	,	,	PUNCT
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eurjchem-1125	127	13	.	.	PUNCT
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eurjchem-1125	128	4	/	/	SYM
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eurjchem-1125	128	9	5	5	NUM
eurjchem-1125	128	10	(	(	PUNCT
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eurjchem-1125	128	13	(	(	PUNCT
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eurjchem-1125	128	15	)	)	PUNCT
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eurjchem-1125	129	2	647	647	NUM
eurjchem-1125	129	3	scheme	scheme	NOUN
eurjchem-1125	129	4	3	3	NUM
eurjchem-1125	129	5	ethyl‐2‐({[2‐({(2e)‐2‐cyano‐3‐[4‐(piperidin‐1‐yl)phenyl	ethyl‐2‐({[2‐({(2e)‐2‐cyano‐3‐[4‐(piperidin‐1‐yl)phenyl	NOUN
eurjchem-1125	129	6	]	]	PUNCT
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eurjchem-1125	129	8	,	,	PUNCT
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eurjchem-1125	129	10	]	]	X
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eurjchem-1125	129	12	,	,	PUNCT
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eurjchem-1125	129	15	(	(	PUNCT
eurjchem-1125	129	16	11	11	NUM
eurjchem-1125	129	17	):	):	PUNCT
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eurjchem-1125	129	19	:	:	PUNCT
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eurjchem-1125	130	2	:	:	PUNCT
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eurjchem-1125	130	5	,	,	PUNCT
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eurjchem-1125	132	4	.	.	PUNCT
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eurjchem-1125	133	2	(	(	PUNCT
eurjchem-1125	133	3	kbr	kbr	PROPN
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eurjchem-1125	133	8	):	):	PUNCT
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eurjchem-1125	134	6	(	(	PUNCT
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eurjchem-1125	134	8	)	)	PUNCT
eurjchem-1125	134	9	):	):	PUNCT
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eurjchem-1125	134	45	)	)	PUNCT
eurjchem-1125	134	46	,	,	PUNCT
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eurjchem-1125	135	4	.	.	PUNCT
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eurjchem-1125	136	5	,	,	PUNCT
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eurjchem-1125	136	9	,	,	PUNCT
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eurjchem-1125	136	17	:	:	PUNCT
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eurjchem-1125	137	2	,	,	PUNCT
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eurjchem-1125	137	4	;	;	PUNCT
eurjchem-1125	137	5	h	h	X
eurjchem-1125	137	6	,	,	PUNCT
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eurjchem-1125	137	8	;	;	PUNCT
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eurjchem-1125	137	12	.	.	PUNCT
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eurjchem-1125	138	3	,	,	PUNCT
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eurjchem-1125	138	5	,	,	PUNCT
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eurjchem-1125	138	7	,	,	PUNCT
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eurjchem-1125	138	9	,	,	PUNCT
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eurjchem-1125	138	13	,	,	PUNCT
eurjchem-1125	138	14	7‐	7‐	NUM
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eurjchem-1125	138	16	(	(	PUNCT
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eurjchem-1125	139	2	:	:	PUNCT
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eurjchem-1125	139	5	,	,	PUNCT
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eurjchem-1125	139	8	.	.	PUNCT
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eurjchem-1125	140	5	°	°	SYM
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eurjchem-1125	140	7	.	.	PUNCT
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eurjchem-1125	141	3	kbr	kbr	PROPN
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eurjchem-1125	141	6	,	,	PUNCT
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eurjchem-1125	141	8	):	):	PUNCT
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eurjchem-1125	141	10	,	,	PUNCT
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eurjchem-1125	141	17	,	,	PUNCT
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eurjchem-1125	141	19	,	,	PUNCT
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eurjchem-1125	142	2	(	(	PUNCT
eurjchem-1125	142	3	m	m	NOUN
eurjchem-1125	142	4	/	/	SYM
eurjchem-1125	142	5	z	z	NOUN
eurjchem-1125	142	6	(	(	PUNCT
eurjchem-1125	142	7	%	%	NOUN
eurjchem-1125	142	8	)	)	PUNCT
eurjchem-1125	142	9	):	):	PUNCT
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eurjchem-1125	142	11	(	(	PUNCT
eurjchem-1125	142	12	m+	m+	NUM
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eurjchem-1125	142	17	,	,	PUNCT
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eurjchem-1125	142	20	m+‐3‐(carbonyliminocoumarine	m+‐3‐(carbonyliminocoumarine	NOUN
eurjchem-1125	142	21	)	)	PUNCT
eurjchem-1125	142	22	,	,	PUNCT
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eurjchem-1125	142	32	,	,	PUNCT
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eurjchem-1125	142	37	,	,	PUNCT
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eurjchem-1125	142	41	)	)	PUNCT
eurjchem-1125	142	42	,	,	PUNCT
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eurjchem-1125	142	44	(	(	PUNCT
eurjchem-1125	142	45	100	100	NUM
eurjchem-1125	142	46	)	)	PUNCT
eurjchem-1125	142	47	,	,	PUNCT
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eurjchem-1125	142	52	,	,	PUNCT
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eurjchem-1125	142	54	(	(	PUNCT
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eurjchem-1125	142	56	)	)	PUNCT
eurjchem-1125	142	57	,	,	PUNCT
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eurjchem-1125	142	61	)	)	PUNCT
eurjchem-1125	142	62	,	,	PUNCT
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eurjchem-1125	142	71	)	)	PUNCT
eurjchem-1125	142	72	,	,	PUNCT
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eurjchem-1125	142	74	(	(	PUNCT
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eurjchem-1125	142	76	)	)	PUNCT
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eurjchem-1125	142	81	)	)	PUNCT
eurjchem-1125	142	82	,	,	PUNCT
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eurjchem-1125	142	84	(	(	PUNCT
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eurjchem-1125	142	86	)	)	PUNCT
eurjchem-1125	142	87	,	,	PUNCT
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eurjchem-1125	142	89	(	(	PUNCT
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eurjchem-1125	142	91	)	)	PUNCT
eurjchem-1125	142	92	.	.	PUNCT
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eurjchem-1125	143	2	.	.	PUNCT
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eurjchem-1125	143	4	.	.	PUNCT
eurjchem-1125	144	1	for	for	ADP
eurjchem-1125	144	2	c30h29n3o5s2	c30h29n3o5s2	ADJ
eurjchem-1125	144	3	:	:	PUNCT
eurjchem-1125	144	4	c	c	X
eurjchem-1125	144	5	,	,	PUNCT
eurjchem-1125	144	6	62.59	62.59	NUM
eurjchem-1125	144	7	;	;	PUNCT
eurjchem-1125	144	8	h	h	X
eurjchem-1125	144	9	,	,	PUNCT
eurjchem-1125	144	10	5.08	5.08	NUM
eurjchem-1125	144	11	;	;	PUNCT
eurjchem-1125	144	12	n	n	CCONJ
eurjchem-1125	144	13	,	,	PUNCT
eurjchem-1125	144	14	7.30	7.30	NUM
eurjchem-1125	144	15	.	.	PUNCT
eurjchem-1125	144	16	found	find	VERB
eurjchem-1125	144	17	:	:	PUNCT
eurjchem-1125	145	1	c	c	X
eurjchem-1125	145	2	,	,	PUNCT
eurjchem-1125	145	3	62.53	62.53	NUM
eurjchem-1125	145	4	;	;	PUNCT
eurjchem-1125	145	5	h	h	NOUN
eurjchem-1125	145	6	,	,	PUNCT
eurjchem-1125	145	7	5.03	5.03	NUM
eurjchem-1125	145	8	;	;	PUNCT
eurjchem-1125	145	9	n	n	CCONJ
eurjchem-1125	145	10	,	,	PUNCT
eurjchem-1125	145	11	7.34	7.34	NUM
eurjchem-1125	145	12	%	%	NOUN
eurjchem-1125	145	13	.	.	PUNCT
eurjchem-1125	146	1	2.2.5	2.2.5	X
eurjchem-1125	146	2	.	.	X
eurjchem-1125	146	3	synthesis	synthesis	NOUN
eurjchem-1125	146	4	of	of	ADP
eurjchem-1125	146	5	ethyl	ethyl	PROPN
eurjchem-1125	146	6	2‐((e)‐2‐cyano‐3‐(4‐((e)‐2‐cyano‐3‐	2‐((e)‐2‐cyano‐3‐(4‐((e)‐2‐cyano‐3‐	PROPN
eurjchem-1125	146	7	(	(	PUNCT
eurjchem-1125	146	8	3‐(ethoxycarbonyl)‐4,5,6	3‐(ethoxycarbonyl)‐4,5,6	NUM
eurjchem-1125	146	9	,	,	PUNCT
eurjchem-1125	146	10	‐tetrahydrobenzo‐[b]thiophen‐2‐	‐tetrahydrobenzo‐[b]thiophen‐2‐	PUNCT
eurjchem-1125	146	11	ylamino)‐3‐oxoprop‐1‐enyl)phenyl)acrylamido)‐4,5,6,7‐	ylamino)‐3‐oxoprop‐1‐enyl)phenyl)acrylamido)‐4,5,6,7‐	PROPN
eurjchem-1125	146	12	tetrahydrobenzo‐[b]thiophene‐3‐carboxylate	tetrahydrobenzo‐[b]thiophene‐3‐carboxylate	PROPN
eurjchem-1125	146	13	(	(	PUNCT
eurjchem-1125	146	14	13	13	NUM
eurjchem-1125	146	15	)	)	PUNCT
eurjchem-1125	146	16	a	a	DET
eurjchem-1125	146	17	mixture	mixture	NOUN
eurjchem-1125	146	18	of	of	ADP
eurjchem-1125	146	19	compound	compound	NOUN
eurjchem-1125	146	20	3	3	NUM
eurjchem-1125	146	21	(	(	PUNCT
eurjchem-1125	146	22	0.73	0.73	NUM
eurjchem-1125	146	23	g	g	NOUN
eurjchem-1125	146	24	,	,	PUNCT
eurjchem-1125	146	25	2.5	2.5	NUM
eurjchem-1125	146	26	mmol	mmol	NOUN
eurjchem-1125	146	27	)	)	PUNCT
eurjchem-1125	146	28	and	and	CCONJ
eurjchem-1125	146	29	terphthal	terphthal	NOUN
eurjchem-1125	146	30	aldehyde	aldehyde	NOUN
eurjchem-1125	146	31	(	(	PUNCT
eurjchem-1125	146	32	0.17	0.17	NUM
eurjchem-1125	146	33	g	g	PART
eurjchem-1125	146	34	1.25	1.25	NUM
eurjchem-1125	146	35	mmol	mmol	NOUN
eurjchem-1125	146	36	)	)	PUNCT
eurjchem-1125	146	37	in	in	ADP
eurjchem-1125	146	38	ethanol	ethanol	NOUN
eurjchem-1125	146	39	(	(	PUNCT
eurjchem-1125	146	40	15	15	NUM
eurjchem-1125	146	41	ml	ml	NOUN
eurjchem-1125	146	42	)	)	PUNCT
eurjchem-1125	146	43	containing	contain	VERB
eurjchem-1125	146	44	piperidine	piperidine	NOUN
eurjchem-1125	146	45	(	(	PUNCT
eurjchem-1125	146	46	0.2	0.2	NUM
eurjchem-1125	146	47	ml	ml	NOUN
eurjchem-1125	146	48	)	)	PUNCT
eurjchem-1125	146	49	was	be	AUX
eurjchem-1125	146	50	stirred	stir	VERB
eurjchem-1125	146	51	at	at	ADP
eurjchem-1125	146	52	80	80	NUM
eurjchem-1125	146	53	°	°	NUM
eurjchem-1125	146	54	c	c	NOUN
eurjchem-1125	146	55	for	for	ADP
eurjchem-1125	146	56	4	4	NUM
eurjchem-1125	146	57	h.	h.	NOUN
eurjchem-1125	146	58	the	the	DET
eurjchem-1125	146	59	separated	separate	VERB
eurjchem-1125	146	60	crystals	crystal	NOUN
eurjchem-1125	146	61	was	be	AUX
eurjchem-1125	146	62	filtered	filter	VERB
eurjchem-1125	146	63	,	,	PUNCT
eurjchem-1125	146	64	dried	dry	VERB
eurjchem-1125	146	65	and	and	CCONJ
eurjchem-1125	146	66	crystallized	crystallize	VERB
eurjchem-1125	146	67	from	from	ADP
eurjchem-1125	146	68	dmf	dmf	PROPN
eurjchem-1125	146	69	:	:	PUNCT
eurjchem-1125	146	70	ethanol	ethanol	NOUN
eurjchem-1125	146	71	(	(	PUNCT
eurjchem-1125	146	72	4:1	4:1	NUM
eurjchem-1125	146	73	,	,	PUNCT
eurjchem-1125	146	74	v	v	NOUN
eurjchem-1125	146	75	:	:	PUNCT
eurjchem-1125	146	76	v	v	NOUN
eurjchem-1125	146	77	)	)	PUNCT
eurjchem-1125	146	78	mixture	mixture	NOUN
eurjchem-1125	146	79	to	to	PART
eurjchem-1125	146	80	give	give	VERB
eurjchem-1125	146	81	compound	compound	NOUN
eurjchem-1125	146	82	13	13	NUM
eurjchem-1125	146	83	(	(	PUNCT
eurjchem-1125	146	84	scheme	scheme	NOUN
eurjchem-1125	146	85	3	3	NUM
eurjchem-1125	146	86	)	)	PUNCT
eurjchem-1125	146	87	.	.	PUNCT
eurjchem-1125	147	1	color	color	NOUN
eurjchem-1125	147	2	:	:	PUNCT
eurjchem-1125	147	3	yellowish	yellowish	VERB
eurjchem-1125	147	4	green	green	ADJ
eurjchem-1125	147	5	powder	powder	NOUN
eurjchem-1125	147	6	.	.	PUNCT
eurjchem-1125	148	1	yield	yield	NOUN
eurjchem-1125	148	2	:	:	PUNCT
eurjchem-1125	148	3	0.56	0.56	NUM
eurjchem-1125	148	4	g	g	NOUN
eurjchem-1125	148	5	,	,	PUNCT
eurjchem-1125	148	6	77	77	NUM
eurjchem-1125	148	7	%	%	NOUN
eurjchem-1125	148	8	.	.	PUNCT
eurjchem-1125	149	1	m.p	m.p	PROPN
eurjchem-1125	149	2	.	.	PROPN
eurjchem-1125	149	3	:	:	PUNCT
eurjchem-1125	150	1	239	239	NUM
eurjchem-1125	150	2	°	°	NUM
eurjchem-1125	150	3	c	c	X
eurjchem-1125	150	4	.	.	PUNCT
eurjchem-1125	151	1	ft‐ir	ft‐ir	NOUN
eurjchem-1125	151	2	(	(	PUNCT
eurjchem-1125	151	3	kbr	kbr	PROPN
eurjchem-1125	151	4	,	,	PUNCT
eurjchem-1125	151	5	ν	ν	PROPN
eurjchem-1125	151	6	,	,	PUNCT
eurjchem-1125	151	7	cm‐1	cm‐1	PROPN
eurjchem-1125	151	8	):	):	PUNCT
eurjchem-1125	151	9	3184	3184	NUM
eurjchem-1125	151	10	,	,	PUNCT
eurjchem-1125	151	11	(	(	PUNCT
eurjchem-1125	151	12	nh	nh	NOUN
eurjchem-1125	151	13	)	)	PUNCT
eurjchem-1125	151	14	,	,	PUNCT
eurjchem-1125	151	15	2195	2195	NUM
eurjchem-1125	151	16	(	(	PUNCT
eurjchem-1125	151	17	cn	cn	PROPN
eurjchem-1125	151	18	)	)	PUNCT
eurjchem-1125	151	19	,	,	PUNCT
eurjchem-1125	151	20	1729	1729	NUM
eurjchem-1125	151	21	,	,	PUNCT
eurjchem-1125	151	22	1677	1677	NUM
eurjchem-1125	151	23	,	,	PUNCT
eurjchem-1125	151	24	1621	1621	NUM
eurjchem-1125	151	25	(	(	PUNCT
eurjchem-1125	151	26	c	c	NOUN
eurjchem-1125	151	27	=	=	NOUN
eurjchem-1125	151	28	o	o	NOUN
eurjchem-1125	151	29	)	)	PUNCT
eurjchem-1125	151	30	.	.	PUNCT
eurjchem-1125	152	1	1h	1h	NUM
eurjchem-1125	152	2	nmr	nmr	NOUN
eurjchem-1125	152	3	(	(	PUNCT
eurjchem-1125	152	4	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	152	5	,	,	PUNCT
eurjchem-1125	152	6	δ	δ	PROPN
eurjchem-1125	152	7	,	,	PUNCT
eurjchem-1125	152	8	ppm	ppm	NUM
eurjchem-1125	152	9	):	):	PUNCT
eurjchem-1125	152	10	1.34	1.34	NUM
eurjchem-1125	152	11	(	(	PUNCT
eurjchem-1125	152	12	m	m	PROPN
eurjchem-1125	152	13	,	,	PUNCT
eurjchem-1125	152	14	6h	6h	NUM
eurjchem-1125	152	15	,	,	PUNCT
eurjchem-1125	152	16	2ch3	2ch3	NUM
eurjchem-1125	152	17	)	)	PUNCT
eurjchem-1125	152	18	,	,	PUNCT
eurjchem-1125	152	19	1.75‐1.82	1.75‐1.82	NUM
eurjchem-1125	152	20	(	(	PUNCT
eurjchem-1125	152	21	m	m	PROPN
eurjchem-1125	152	22	,	,	PUNCT
eurjchem-1125	152	23	8h	8h	NUM
eurjchem-1125	152	24	,	,	PUNCT
eurjchem-1125	152	25	2c5‐2h	2c5‐2h	NUM
eurjchem-1125	152	26	,	,	PUNCT
eurjchem-1125	152	27	2c6‐2h	2c6‐2h	NUM
eurjchem-1125	152	28	,	,	PUNCT
eurjchem-1125	152	29	cyclohexane	cyclohexane	NOUN
eurjchem-1125	152	30	skeleton	skeleton	NOUN
eurjchem-1125	152	31	)	)	PUNCT
eurjchem-1125	152	32	,	,	PUNCT
eurjchem-1125	152	33	2.82‐3.12	2.82‐3.12	NUM
eurjchem-1125	152	34	(	(	PUNCT
eurjchem-1125	152	35	m	m	PROPN
eurjchem-1125	152	36	,	,	PUNCT
eurjchem-1125	152	37	8h	8h	NUM
eurjchem-1125	152	38	,	,	PUNCT
eurjchem-1125	152	39	2c4‐2h	2c4‐2h	NUM
eurjchem-1125	152	40	,	,	PUNCT
eurjchem-1125	152	41	2c7‐2h	2c7‐2h	NUM
eurjchem-1125	152	42	,	,	PUNCT
eurjchem-1125	152	43	cyclohexane	cyclohexane	NOUN
eurjchem-1125	152	44	skeleton	skeleton	NOUN
eurjchem-1125	152	45	)	)	PUNCT
eurjchem-1125	152	46	,	,	PUNCT
eurjchem-1125	152	47	4.42	4.42	NUM
eurjchem-1125	152	48	(	(	PUNCT
eurjchem-1125	152	49	m	m	PROPN
eurjchem-1125	152	50	,	,	PUNCT
eurjchem-1125	152	51	4h	4h	NUM
eurjchem-1125	152	52	,	,	PUNCT
eurjchem-1125	152	53	2ch2o	2ch2o	NUM
eurjchem-1125	152	54	)	)	PUNCT
eurjchem-1125	152	55	,	,	PUNCT
eurjchem-1125	152	56	7.70‐8.0	7.70‐8.0	PROPN
eurjchem-1125	152	57	(	(	PUNCT
eurjchem-1125	152	58	m	m	PROPN
eurjchem-1125	152	59	,	,	PUNCT
eurjchem-1125	152	60	6h	6h	NUM
eurjchem-1125	152	61	,	,	PUNCT
eurjchem-1125	152	62	ar‐h	ar‐h	NOUN
eurjchem-1125	152	63	,	,	PUNCT
eurjchem-1125	152	64	2ch=	2ch=	NOUN
eurjchem-1125	152	65	)	)	PUNCT
eurjchem-1125	152	66	,	,	PUNCT
eurjchem-1125	152	67	11.45	11.45	NUM
eurjchem-1125	152	68	(	(	PUNCT
eurjchem-1125	152	69	s	s	PROPN
eurjchem-1125	152	70	,	,	PUNCT
eurjchem-1125	152	71	1h	1h	NUM
eurjchem-1125	152	72	,	,	PUNCT
eurjchem-1125	152	73	nh‐co	nh‐co	NUM
eurjchem-1125	152	74	)	)	PUNCT
eurjchem-1125	152	75	,	,	PUNCT
eurjchem-1125	152	76	11.75	11.75	NUM
eurjchem-1125	152	77	(	(	PUNCT
eurjchem-1125	152	78	s	s	PROPN
eurjchem-1125	152	79	,	,	PUNCT
eurjchem-1125	152	80	1h	1h	NUM
eurjchem-1125	152	81	,	,	PUNCT
eurjchem-1125	152	82	nh‐co	nh‐co	NUM
eurjchem-1125	152	83	)	)	PUNCT
eurjchem-1125	152	84	.	.	PUNCT
eurjchem-1125	153	1	ei‐ms	ei‐ms	PROPN
eurjchem-1125	153	2	(	(	PUNCT
eurjchem-1125	153	3	m	m	NOUN
eurjchem-1125	153	4	/	/	SYM
eurjchem-1125	153	5	z	z	NOUN
eurjchem-1125	153	6	(	(	PUNCT
eurjchem-1125	153	7	%	%	NOUN
eurjchem-1125	153	8	)	)	PUNCT
eurjchem-1125	153	9	):	):	PUNCT
eurjchem-1125	153	10	679	679	NUM
eurjchem-1125	153	11	(	(	PUNCT
eurjchem-1125	153	12	m+‐3	m+‐3	NOUN
eurjchem-1125	153	13	,	,	PUNCT
eurjchem-1125	153	14	0.1	0.1	NUM
eurjchem-1125	153	15	)	)	PUNCT
eurjchem-1125	153	16	,	,	PUNCT
eurjchem-1125	153	17	543	543	NUM
eurjchem-1125	153	18	(	(	PUNCT
eurjchem-1125	153	19	0.2	0.2	NUM
eurjchem-1125	153	20	)	)	PUNCT
eurjchem-1125	153	21	,	,	PUNCT
eurjchem-1125	153	22	499	499	NUM
eurjchem-1125	153	23	(	(	PUNCT
eurjchem-1125	153	24	0.2	0.2	NUM
eurjchem-1125	153	25	)	)	PUNCT
eurjchem-1125	153	26	,	,	PUNCT
eurjchem-1125	153	27	453	453	NUM
eurjchem-1125	153	28	(	(	PUNCT
eurjchem-1125	153	29	0.2	0.2	NUM
eurjchem-1125	153	30	)	)	PUNCT
eurjchem-1125	153	31	,	,	PUNCT
eurjchem-1125	153	32	404	404	NUM
eurjchem-1125	153	33	(	(	PUNCT
eurjchem-1125	153	34	0.3	0.3	NUM
eurjchem-1125	153	35	)	)	PUNCT
eurjchem-1125	153	36	,	,	PUNCT
eurjchem-1125	153	37	384	384	NUM
eurjchem-1125	153	38	(	(	PUNCT
eurjchem-1125	153	39	1.2	1.2	NUM
eurjchem-1125	153	40	)	)	PUNCT
eurjchem-1125	153	41	,	,	PUNCT
eurjchem-1125	153	42	359	359	NUM
eurjchem-1125	153	43	(	(	PUNCT
eurjchem-1125	153	44	7.8	7.8	NUM
eurjchem-1125	153	45	)	)	PUNCT
eurjchem-1125	153	46	,	,	PUNCT
eurjchem-1125	153	47	336	336	NUM
eurjchem-1125	153	48	(	(	PUNCT
eurjchem-1125	153	49	19.3	19.3	NUM
eurjchem-1125	153	50	)	)	PUNCT
eurjchem-1125	153	51	,	,	PUNCT
eurjchem-1125	153	52	290	290	NUM
eurjchem-1125	153	53	(	(	PUNCT
eurjchem-1125	153	54	8.9	8.9	NUM
eurjchem-1125	153	55	)	)	PUNCT
eurjchem-1125	153	56	,	,	PUNCT
eurjchem-1125	153	57	246	246	NUM
eurjchem-1125	153	58	(	(	PUNCT
eurjchem-1125	153	59	21.5	21.5	NUM
eurjchem-1125	153	60	)	)	PUNCT
eurjchem-1125	153	61	,	,	PUNCT
eurjchem-1125	153	62	224	224	NUM
eurjchem-1125	153	63	(	(	PUNCT
eurjchem-1125	153	64	27.4	27.4	NUM
eurjchem-1125	153	65	)	)	PUNCT
eurjchem-1125	153	66	,	,	PUNCT
eurjchem-1125	153	67	205	205	NUM
eurjchem-1125	153	68	(	(	PUNCT
eurjchem-1125	153	69	33.4	33.4	NUM
eurjchem-1125	153	70	)	)	PUNCT
eurjchem-1125	153	71	,	,	PUNCT
eurjchem-1125	153	72	178	178	NUM
eurjchem-1125	153	73	(	(	PUNCT
eurjchem-1125	153	74	70.0	70.0	NUM
eurjchem-1125	153	75	)	)	PUNCT
eurjchem-1125	153	76	,	,	PUNCT
eurjchem-1125	153	77	150	150	NUM
eurjchem-1125	153	78	(	(	PUNCT
eurjchem-1125	153	79	91.3	91.3	NUM
eurjchem-1125	153	80	)	)	PUNCT
eurjchem-1125	153	81	,	,	PUNCT
eurjchem-1125	153	82	126	126	NUM
eurjchem-1125	153	83	(	(	PUNCT
eurjchem-1125	153	84	43.9	43.9	NUM
eurjchem-1125	153	85	)	)	PUNCT
eurjchem-1125	153	86	,	,	PUNCT
eurjchem-1125	153	87	122	122	NUM
eurjchem-1125	153	88	(	(	PUNCT
eurjchem-1125	153	89	72.9	72.9	NUM
eurjchem-1125	153	90	)	)	PUNCT
eurjchem-1125	153	91	,	,	PUNCT
eurjchem-1125	153	92	111	111	NUM
eurjchem-1125	153	93	(	(	PUNCT
eurjchem-1125	153	94	82.8	82.8	NUM
eurjchem-1125	153	95	)	)	PUNCT
eurjchem-1125	153	96	,	,	PUNCT
eurjchem-1125	153	97	90(60.0	90(60.0	NOUN
eurjchem-1125	153	98	)	)	PUNCT
eurjchem-1125	153	99	,	,	PUNCT
eurjchem-1125	153	100	83(72.1	83(72.1	NOUN
eurjchem-1125	153	101	)	)	PUNCT
eurjchem-1125	153	102	,	,	PUNCT
eurjchem-1125	153	103	68	68	NUM
eurjchem-1125	153	104	(	(	PUNCT
eurjchem-1125	153	105	100	100	NUM
eurjchem-1125	153	106	)	)	PUNCT
eurjchem-1125	153	107	.	.	PUNCT
eurjchem-1125	154	1	anal	anal	PROPN
eurjchem-1125	154	2	.	.	PUNCT
eurjchem-1125	154	3	calcd	calcd	NOUN
eurjchem-1125	154	4	.	.	PUNCT
eurjchem-1125	155	1	for	for	ADP
eurjchem-1125	155	2	c36h34n4o6s2	c36h34n4o6s2	NOUN
eurjchem-1125	155	3	:	:	PUNCT
eurjchem-1125	155	4	c	c	X
eurjchem-1125	155	5	,	,	PUNCT
eurjchem-1125	155	6	63.32	63.32	NUM
eurjchem-1125	155	7	;	;	PUNCT
eurjchem-1125	155	8	h	h	NOUN
eurjchem-1125	155	9	,	,	PUNCT
eurjchem-1125	155	10	5.02	5.02	NUM
eurjchem-1125	155	11	;	;	PUNCT
eurjchem-1125	155	12	n	n	CCONJ
eurjchem-1125	155	13	,	,	PUNCT
eurjchem-1125	155	14	8.21	8.21	NUM
eurjchem-1125	155	15	.	.	PUNCT
eurjchem-1125	155	16	found	find	VERB
eurjchem-1125	155	17	:	:	PUNCT
eurjchem-1125	156	1	c	c	X
eurjchem-1125	156	2	,	,	PUNCT
eurjchem-1125	156	3	63.41	63.41	NUM
eurjchem-1125	156	4	;	;	PUNCT
eurjchem-1125	156	5	h	h	NOUN
eurjchem-1125	156	6	,	,	PUNCT
eurjchem-1125	156	7	5.06	5.06	NUM
eurjchem-1125	156	8	;	;	PUNCT
eurjchem-1125	156	9	n	n	CCONJ
eurjchem-1125	156	10	,	,	PUNCT
eurjchem-1125	156	11	8.23	8.23	NUM
eurjchem-1125	156	12	%	%	NOUN
eurjchem-1125	156	13	.	.	PUNCT
eurjchem-1125	157	1	2.2.6	2.2.6	X
eurjchem-1125	157	2	.	.	PUNCT
eurjchem-1125	158	1	synthesis	synthesis	NOUN
eurjchem-1125	158	2	of	of	ADP
eurjchem-1125	158	3	ethyl‐(e)‐2‐cyano‐2‐(2‐(4‐((e)‐2‐cyano‐1‐	ethyl‐(e)‐2‐cyano‐2‐(2‐(4‐((e)‐2‐cyano‐1‐	NOUN
eurjchem-1125	158	4	(	(	PUNCT
eurjchem-1125	158	5	3‐(ethoxycarbonyl)‐4,5,6,7‐tetrahydrobenzo[b]thiophen‐2‐	3‐(ethoxycarbonyl)‐4,5,6,7‐tetrahydrobenzo[b]thiophen‐2‐	NUM
eurjchem-1125	158	6	ylacetamido)hydrazono)phenylhydrazono)‐n‐(4,5,6,7‐tetra	ylacetamido)hydrazono)phenylhydrazono)‐n‐(4,5,6,7‐tetra	NOUN
eurjchem-1125	158	7	hydrobenzo	hydrobenzo	NOUN
eurjchem-1125	158	8	[	[	X
eurjchem-1125	158	9	b]thiophen‐2‐yl)acetamido‐3‐	b]thiophen‐2‐yl)acetamido‐3‐	ADJ
eurjchem-1125	158	10	carboxylate	carboxylate	NOUN
eurjchem-1125	158	11	(	(	PUNCT
eurjchem-1125	158	12	14	14	NUM
eurjchem-1125	158	13	)	)	PUNCT
eurjchem-1125	158	14	to	to	ADP
eurjchem-1125	158	15	a	a	DET
eurjchem-1125	158	16	well	well	ADV
eurjchem-1125	158	17	stirred	stir	VERB
eurjchem-1125	158	18	cooled	cool	VERB
eurjchem-1125	158	19	solution	solution	NOUN
eurjchem-1125	158	20	of	of	ADP
eurjchem-1125	158	21	p‐phenylenediamine	p‐phenylenediamine	PUNCT
eurjchem-1125	158	22	(	(	PUNCT
eurjchem-1125	158	23	0.27	0.27	NUM
eurjchem-1125	158	24	g	g	NOUN
eurjchem-1125	158	25	,	,	PUNCT
eurjchem-1125	158	26	2.5	2.5	NUM
eurjchem-1125	158	27	mmol	mmol	NOUN
eurjchem-1125	158	28	)	)	PUNCT
eurjchem-1125	158	29	in	in	ADP
eurjchem-1125	158	30	conc	conc	NOUN
eurjchem-1125	158	31	.	.	PUNCT
eurjchem-1125	159	1	hcl	hcl	PROPN
eurjchem-1125	159	2	(	(	PUNCT
eurjchem-1125	159	3	3	3	NUM
eurjchem-1125	159	4	ml	ml	NOUN
eurjchem-1125	159	5	)	)	PUNCT
eurjchem-1125	159	6	,	,	PUNCT
eurjchem-1125	159	7	a	a	DET
eurjchem-1125	159	8	solution	solution	NOUN
eurjchem-1125	159	9	of	of	ADP
eurjchem-1125	159	10	nano2	nano2	NOUN
eurjchem-1125	159	11	(	(	PUNCT
eurjchem-1125	159	12	0.4	0.4	NUM
eurjchem-1125	159	13	g	g	NOUN
eurjchem-1125	159	14	,	,	PUNCT
eurjchem-1125	159	15	5.8	5.8	NUM
eurjchem-1125	159	16	mmol	mmol	NOUN
eurjchem-1125	159	17	in	in	ADP
eurjchem-1125	159	18	5	5	NUM
eurjchem-1125	159	19	ml	ml	X
eurjchem-1125	159	20	h2o	h2o	PROPN
eurjchem-1125	159	21	)	)	PUNCT
eurjchem-1125	159	22	was	be	AUX
eurjchem-1125	159	23	added	add	VERB
eurjchem-1125	159	24	dropwise	dropwise	NOUN
eurjchem-1125	159	25	.	.	PUNCT
eurjchem-1125	160	1	the	the	DET
eurjchem-1125	160	2	above	above	ADJ
eurjchem-1125	160	3	cooled	cooled	ADJ
eurjchem-1125	160	4	diazonium	diazonium	NOUN
eurjchem-1125	160	5	salt	salt	NOUN
eurjchem-1125	160	6	solution	solution	NOUN
eurjchem-1125	160	7	was	be	AUX
eurjchem-1125	160	8	added	add	VERB
eurjchem-1125	160	9	slowly	slowly	ADV
eurjchem-1125	160	10	to	to	ADP
eurjchem-1125	160	11	a	a	DET
eurjchem-1125	160	12	well	well	ADV
eurjchem-1125	160	13	stirred	stir	VERB
eurjchem-1125	160	14	solution	solution	NOUN
eurjchem-1125	160	15	of	of	ADP
eurjchem-1125	160	16	2	2	NUM
eurjchem-1125	160	17	(	(	PUNCT
eurjchem-1125	160	18	1.46	1.46	NUM
eurjchem-1125	160	19	g	g	NOUN
eurjchem-1125	160	20	,	,	PUNCT
eurjchem-1125	160	21	5	5	NUM
eurjchem-1125	160	22	mmol	mmol	NOUN
eurjchem-1125	160	23	)	)	PUNCT
eurjchem-1125	160	24	in	in	ADP
eurjchem-1125	160	25	pyridine	pyridine	NOUN
eurjchem-1125	160	26	(	(	PUNCT
eurjchem-1125	160	27	20	20	NUM
eurjchem-1125	160	28	ml	ml	NOUN
eurjchem-1125	160	29	)	)	PUNCT
eurjchem-1125	160	30	.	.	PUNCT
eurjchem-1125	161	1	the	the	DET
eurjchem-1125	161	2	reaction	reaction	NOUN
eurjchem-1125	161	3	mixture	mixture	NOUN
eurjchem-1125	161	4	was	be	AUX
eurjchem-1125	161	5	stirred	stir	VERB
eurjchem-1125	161	6	for	for	ADP
eurjchem-1125	161	7	2	2	NUM
eurjchem-1125	161	8	h.	h.	NOUN
eurjchem-1125	161	9	the	the	DET
eurjchem-1125	161	10	crude	crude	ADJ
eurjchem-1125	161	11	product	product	NOUN
eurjchem-1125	161	12	was	be	AUX
eurjchem-1125	161	13	filtered	filter	VERB
eurjchem-1125	161	14	off	off	ADP
eurjchem-1125	161	15	,	,	PUNCT
eurjchem-1125	161	16	dried	dry	VERB
eurjchem-1125	161	17	and	and	CCONJ
eurjchem-1125	161	18	recrystallize	recrystallize	NOUN
eurjchem-1125	161	19	from	from	ADP
eurjchem-1125	161	20	dmf	dmf	PROPN
eurjchem-1125	161	21	:	:	PUNCT
eurjchem-1125	161	22	etoh	etoh	NOUN
eurjchem-1125	161	23	(	(	PUNCT
eurjchem-1125	161	24	5:2	5:2	NUM
eurjchem-1125	161	25	,	,	PUNCT
eurjchem-1125	161	26	v	v	NOUN
eurjchem-1125	161	27	:	:	PUNCT
eurjchem-1125	161	28	v	v	NOUN
eurjchem-1125	161	29	)	)	PUNCT
eurjchem-1125	161	30	mixture	mixture	NOUN
eurjchem-1125	161	31	to	to	PART
eurjchem-1125	161	32	give	give	VERB
eurjchem-1125	161	33	compound	compound	NOUN
eurjchem-1125	161	34	14	14	NUM
eurjchem-1125	161	35	(	(	PUNCT
eurjchem-1125	161	36	scheme	scheme	NOUN
eurjchem-1125	161	37	3	3	NUM
eurjchem-1125	161	38	)	)	PUNCT
eurjchem-1125	161	39	.	.	PUNCT
eurjchem-1125	162	1	color	color	NOUN
eurjchem-1125	162	2	:	:	PUNCT
eurjchem-1125	162	3	scarlet	scarlet	ADJ
eurjchem-1125	162	4	red	red	ADJ
eurjchem-1125	162	5	crystals	crystal	NOUN
eurjchem-1125	162	6	.	.	PUNCT
eurjchem-1125	163	1	yield	yield	NOUN
eurjchem-1125	163	2	:	:	PUNCT
eurjchem-1125	163	3	1.57	1.57	NUM
eurjchem-1125	163	4	g	g	NOUN
eurjchem-1125	163	5	,	,	PUNCT
eurjchem-1125	163	6	88	88	NUM
eurjchem-1125	163	7	%	%	NOUN
eurjchem-1125	163	8	.	.	PUNCT
eurjchem-1125	164	1	m.p	m.p	PROPN
eurjchem-1125	164	2	.	.	PROPN
eurjchem-1125	164	3	:	:	PUNCT
eurjchem-1125	165	1	305	305	NUM
eurjchem-1125	165	2	°	°	SYM
eurjchem-1125	165	3	c	c	X
eurjchem-1125	165	4	.	.	PUNCT
eurjchem-1125	166	1	ft‐ir	ft‐ir	NOUN
eurjchem-1125	166	2	(	(	PUNCT
eurjchem-1125	166	3	kbr	kbr	PROPN
eurjchem-1125	166	4	,	,	PUNCT
eurjchem-1125	166	5	ν	ν	PROPN
eurjchem-1125	166	6	,	,	PUNCT
eurjchem-1125	166	7	cm‐1	cm‐1	PROPN
eurjchem-1125	166	8	):	):	PUNCT
eurjchem-1125	166	9	3218	3218	NUM
eurjchem-1125	166	10	,	,	PUNCT
eurjchem-1125	166	11	3166	3166	NUM
eurjchem-1125	166	12	(	(	PUNCT
eurjchem-1125	166	13	nh	nh	NOUN
eurjchem-1125	166	14	)	)	PUNCT
eurjchem-1125	166	15	,	,	PUNCT
eurjchem-1125	166	16	2220	2220	NUM
eurjchem-1125	166	17	,	,	PUNCT
eurjchem-1125	166	18	(	(	PUNCT
eurjchem-1125	166	19	cn	cn	PROPN
eurjchem-1125	166	20	)	)	PUNCT
eurjchem-1125	166	21	,	,	PUNCT
eurjchem-1125	166	22	1666	1666	NUM
eurjchem-1125	166	23	,	,	PUNCT
eurjchem-1125	166	24	1625	1625	NUM
eurjchem-1125	166	25	(	(	PUNCT
eurjchem-1125	166	26	c	c	NOUN
eurjchem-1125	166	27	=	=	NOUN
eurjchem-1125	166	28	o	o	NOUN
eurjchem-1125	166	29	)	)	PUNCT
eurjchem-1125	166	30	,	,	PUNCT
eurjchem-1125	166	31	1488	1488	NUM
eurjchem-1125	166	32	(	(	PUNCT
eurjchem-1125	166	33	n	n	CCONJ
eurjchem-1125	166	34	=	=	NUM
eurjchem-1125	166	35	n	n	NUM
eurjchem-1125	166	36	)	)	PUNCT
eurjchem-1125	166	37	.	.	PUNCT
eurjchem-1125	167	1	1h	1h	NUM
eurjchem-1125	167	2	nmr	nmr	NOUN
eurjchem-1125	167	3	(	(	PUNCT
eurjchem-1125	167	4	400	400	NUM
eurjchem-1125	167	5	mhz	mhz	NOUN
eurjchem-1125	167	6	,	,	PUNCT
eurjchem-1125	167	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	167	8	,	,	PUNCT
eurjchem-1125	167	9	δ	δ	PROPN
eurjchem-1125	167	10	,	,	PUNCT
eurjchem-1125	167	11	ppm	ppm	NUM
eurjchem-1125	167	12	):	):	PUNCT
eurjchem-1125	167	13	1.38‐1.41	1.38‐1.41	NUM
eurjchem-1125	167	14	(	(	PUNCT
eurjchem-1125	167	15	m	m	PROPN
eurjchem-1125	167	16	,	,	PUNCT
eurjchem-1125	167	17	6h	6h	NUM
eurjchem-1125	167	18	,	,	PUNCT
eurjchem-1125	167	19	2ch3	2ch3	NUM
eurjchem-1125	167	20	)	)	PUNCT
eurjchem-1125	167	21	,	,	PUNCT
eurjchem-1125	167	22	1.76‐1.82	1.76‐1.82	NUM
eurjchem-1125	167	23	(	(	PUNCT
eurjchem-1125	167	24	m	m	PROPN
eurjchem-1125	167	25	,	,	PUNCT
eurjchem-1125	167	26	8h	8h	NUM
eurjchem-1125	167	27	,	,	PUNCT
eurjchem-1125	167	28	2c5‐2h	2c5‐2h	NUM
eurjchem-1125	167	29	,	,	PUNCT
eurjchem-1125	167	30	2c6‐2h	2c6‐2h	NUM
eurjchem-1125	167	31	,	,	PUNCT
eurjchem-1125	167	32	cyclohexane	cyclohexane	NOUN
eurjchem-1125	167	33	skeleton	skeleton	NOUN
eurjchem-1125	167	34	)	)	PUNCT
eurjchem-1125	167	35	,	,	PUNCT
eurjchem-1125	167	36	2.70‐	2.70‐	NUM
eurjchem-1125	167	37	2.93	2.93	NUM
eurjchem-1125	167	38	(	(	PUNCT
eurjchem-1125	167	39	m	m	PROPN
eurjchem-1125	167	40	,	,	PUNCT
eurjchem-1125	167	41	8h	8h	NUM
eurjchem-1125	167	42	,	,	PUNCT
eurjchem-1125	167	43	2c4‐2h	2c4‐2h	NUM
eurjchem-1125	167	44	,	,	PUNCT
eurjchem-1125	167	45	2c7‐2h	2c7‐2h	NUM
eurjchem-1125	167	46	,	,	PUNCT
eurjchem-1125	167	47	cyclohexane	cyclohexane	NOUN
eurjchem-1125	167	48	skeleton	skeleton	NOUN
eurjchem-1125	167	49	)	)	PUNCT
eurjchem-1125	167	50	,	,	PUNCT
eurjchem-1125	167	51	4.41‐4.43	4.41‐4.43	NUM
eurjchem-1125	167	52	(	(	PUNCT
eurjchem-1125	167	53	m	m	PROPN
eurjchem-1125	167	54	,	,	PUNCT
eurjchem-1125	167	55	4h	4h	NUM
eurjchem-1125	167	56	,	,	PUNCT
eurjchem-1125	167	57	2ch2o	2ch2o	NUM
eurjchem-1125	167	58	)	)	PUNCT
eurjchem-1125	167	59	,	,	PUNCT
eurjchem-1125	167	60	7.93‐8.44	7.93‐8.44	NUM
eurjchem-1125	167	61	(	(	PUNCT
eurjchem-1125	167	62	m	m	PROPN
eurjchem-1125	167	63	,	,	PUNCT
eurjchem-1125	167	64	4h	4h	NOUN
eurjchem-1125	167	65	,	,	PUNCT
eurjchem-1125	167	66	ar‐h	ar‐h	PROPN
eurjchem-1125	167	67	)	)	PUNCT
eurjchem-1125	167	68	,	,	PUNCT
eurjchem-1125	167	69	10.45	10.45	NUM
eurjchem-1125	167	70	(	(	PUNCT
eurjchem-1125	167	71	s	s	PROPN
eurjchem-1125	167	72	,	,	PUNCT
eurjchem-1125	167	73	1h	1h	NUM
eurjchem-1125	167	74	,	,	PUNCT
eurjchem-1125	167	75	nh‐co	nh‐co	NUM
eurjchem-1125	167	76	)	)	PUNCT
eurjchem-1125	167	77	,	,	PUNCT
eurjchem-1125	167	78	10.65	10.65	NUM
eurjchem-1125	167	79	(	(	PUNCT
eurjchem-1125	167	80	s	s	PROPN
eurjchem-1125	167	81	,	,	PUNCT
eurjchem-1125	167	82	1h	1h	NUM
eurjchem-1125	167	83	,	,	PUNCT
eurjchem-1125	167	84	nh‐co	nh‐co	NUM
eurjchem-1125	167	85	)	)	PUNCT
eurjchem-1125	167	86	,	,	PUNCT
eurjchem-1125	167	87	12.45	12.45	NUM
eurjchem-1125	167	88	(	(	PUNCT
eurjchem-1125	167	89	br	br	PROPN
eurjchem-1125	167	90	,	,	PUNCT
eurjchem-1125	167	91	1h	1h	NUM
eurjchem-1125	167	92	,	,	PUNCT
eurjchem-1125	167	93	nh	nh	PROPN
eurjchem-1125	167	94	=	=	NOUN
eurjchem-1125	167	95	n	n	CCONJ
eurjchem-1125	167	96	)	)	PUNCT
eurjchem-1125	167	97	,	,	PUNCT
eurjchem-1125	167	98	12.54	12.54	NUM
eurjchem-1125	167	99	(	(	PUNCT
eurjchem-1125	167	100	br	br	PROPN
eurjchem-1125	167	101	,	,	PUNCT
eurjchem-1125	167	102	1h	1h	NUM
eurjchem-1125	167	103	,	,	PUNCT
eurjchem-1125	167	104	nh	nh	PROPN
eurjchem-1125	167	105	=	=	NOUN
eurjchem-1125	167	106	n	n	NUM
eurjchem-1125	167	107	)	)	PUNCT
eurjchem-1125	167	108	.	.	PUNCT
eurjchem-1125	168	1	ei‐ms	ei‐ms	PROPN
eurjchem-1125	168	2	(	(	PUNCT
eurjchem-1125	168	3	m	m	NOUN
eurjchem-1125	168	4	/	/	SYM
eurjchem-1125	168	5	z	z	NOUN
eurjchem-1125	168	6	(	(	PUNCT
eurjchem-1125	168	7	%	%	NOUN
eurjchem-1125	168	8	)	)	PUNCT
eurjchem-1125	168	9	):	):	PUNCT
eurjchem-1125	168	10	723	723	NUM
eurjchem-1125	168	11	(	(	PUNCT
eurjchem-1125	168	12	m++1/2h2o	m++1/2h2o	NOUN
eurjchem-1125	168	13	,	,	PUNCT
eurjchem-1125	168	14	0.1	0.1	NUM
eurjchem-1125	168	15	)	)	PUNCT
eurjchem-1125	168	16	,	,	PUNCT
eurjchem-1125	168	17	513	513	NUM
eurjchem-1125	168	18	(	(	PUNCT
eurjchem-1125	168	19	m+	m+	NUM
eurjchem-1125	168	20	,	,	PUNCT
eurjchem-1125	168	21	0.2	0.2	NUM
eurjchem-1125	168	22	)	)	PUNCT
eurjchem-1125	168	23	,	,	PUNCT
eurjchem-1125	168	24	467	467	NUM
eurjchem-1125	168	25	(	(	PUNCT
eurjchem-1125	168	26	0.6	0.6	NUM
eurjchem-1125	168	27	)	)	PUNCT
eurjchem-1125	168	28	,	,	PUNCT
eurjchem-1125	168	29	436	436	NUM
eurjchem-1125	168	30	(	(	PUNCT
eurjchem-1125	168	31	0.8	0.8	NUM
eurjchem-1125	168	32	)	)	PUNCT
eurjchem-1125	168	33	,	,	PUNCT
eurjchem-1125	168	34	396	396	NUM
eurjchem-1125	168	35	(	(	PUNCT
eurjchem-1125	168	36	5.5	5.5	NUM
eurjchem-1125	168	37	)	)	PUNCT
eurjchem-1125	168	38	,	,	PUNCT
eurjchem-1125	168	39	292	292	NUM
eurjchem-1125	168	40	(	(	PUNCT
eurjchem-1125	168	41	10.1	10.1	NUM
eurjchem-1125	168	42	)	)	PUNCT
eurjchem-1125	168	43	,	,	PUNCT
eurjchem-1125	168	44	246	246	NUM
eurjchem-1125	168	45	(	(	PUNCT
eurjchem-1125	168	46	28.7	28.7	NUM
eurjchem-1125	168	47	)	)	PUNCT
eurjchem-1125	168	48	,	,	PUNCT
eurjchem-1125	168	49	225	225	NUM
eurjchem-1125	168	50	(	(	PUNCT
eurjchem-1125	168	51	27.5	27.5	NUM
eurjchem-1125	168	52	)	)	PUNCT
eurjchem-1125	168	53	,	,	PUNCT
eurjchem-1125	168	54	206	206	NUM
eurjchem-1125	168	55	(	(	PUNCT
eurjchem-1125	168	56	91.4	91.4	NUM
eurjchem-1125	168	57	)	)	PUNCT
eurjchem-1125	168	58	,	,	PUNCT
eurjchem-1125	168	59	178	178	NUM
eurjchem-1125	168	60	(	(	PUNCT
eurjchem-1125	168	61	100	100	NUM
eurjchem-1125	168	62	)	)	PUNCT
eurjchem-1125	168	63	,	,	PUNCT
eurjchem-1125	168	64	150	150	NUM
eurjchem-1125	168	65	(	(	PUNCT
eurjchem-1125	168	66	65.0	65.0	NUM
eurjchem-1125	168	67	)	)	PUNCT
eurjchem-1125	168	68	,	,	PUNCT
eurjchem-1125	168	69	121	121	NUM
eurjchem-1125	168	70	(	(	PUNCT
eurjchem-1125	168	71	44.3	44.3	NUM
eurjchem-1125	168	72	)	)	PUNCT
eurjchem-1125	168	73	,	,	PUNCT
eurjchem-1125	168	74	115	115	NUM
eurjchem-1125	168	75	(	(	PUNCT
eurjchem-1125	168	76	38.0	38.0	NUM
eurjchem-1125	168	77	)	)	PUNCT
eurjchem-1125	168	78	,	,	PUNCT
eurjchem-1125	168	79	104	104	NUM
eurjchem-1125	168	80	(	(	PUNCT
eurjchem-1125	168	81	31.9	31.9	NUM
eurjchem-1125	168	82	)	)	PUNCT
eurjchem-1125	168	83	,	,	PUNCT
eurjchem-1125	168	84	90	90	NUM
eurjchem-1125	168	85	(	(	PUNCT
eurjchem-1125	168	86	65.5	65.5	NUM
eurjchem-1125	168	87	)	)	PUNCT
eurjchem-1125	168	88	,	,	PUNCT
eurjchem-1125	168	89	67	67	NUM
eurjchem-1125	168	90	(	(	PUNCT
eurjchem-1125	168	91	65.3	65.3	NUM
eurjchem-1125	168	92	)	)	PUNCT
eurjchem-1125	168	93	,	,	PUNCT
eurjchem-1125	168	94	64	64	NUM
eurjchem-1125	168	95	(	(	PUNCT
eurjchem-1125	168	96	52.9	52.9	NUM
eurjchem-1125	168	97	)	)	PUNCT
eurjchem-1125	168	98	.	.	PUNCT
eurjchem-1125	169	1	anal	anal	PROPN
eurjchem-1125	169	2	.	.	PUNCT
eurjchem-1125	169	3	calcd	calcd	NOUN
eurjchem-1125	169	4	.	.	PUNCT
eurjchem-1125	170	1	for	for	SCONJ
eurjchem-1125	170	2	c34h34n8o6s2	c34h34n8o6s2	ADJ
eurjchem-1125	170	3	:	:	PUNCT
eurjchem-1125	170	4	c	c	X
eurjchem-1125	170	5	,	,	PUNCT
eurjchem-1125	170	6	57.13	57.13	NUM
eurjchem-1125	170	7	;	;	PUNCT
eurjchem-1125	170	8	h	h	NOUN
eurjchem-1125	170	9	,	,	PUNCT
eurjchem-1125	170	10	4.79	4.79	NUM
eurjchem-1125	170	11	;	;	PUNCT
eurjchem-1125	170	12	n	n	CCONJ
eurjchem-1125	170	13	,	,	PUNCT
eurjchem-1125	170	14	15.68	15.68	NUM
eurjchem-1125	170	15	.	.	PUNCT
eurjchem-1125	170	16	found	find	VERB
eurjchem-1125	170	17	:	:	PUNCT
eurjchem-1125	171	1	c	c	X
eurjchem-1125	171	2	,	,	PUNCT
eurjchem-1125	171	3	57.18	57.18	NUM
eurjchem-1125	171	4	;	;	PUNCT
eurjchem-1125	171	5	h	h	NOUN
eurjchem-1125	171	6	,	,	PUNCT
eurjchem-1125	171	7	4.73	4.73	NUM
eurjchem-1125	171	8	;	;	PUNCT
eurjchem-1125	171	9	n	n	CCONJ
eurjchem-1125	171	10	,	,	PUNCT
eurjchem-1125	171	11	15.62	15.62	NUM
eurjchem-1125	171	12	%	%	NOUN
eurjchem-1125	171	13	.	.	PUNCT
eurjchem-1125	172	1	2.2.7	2.2.7	X
eurjchem-1125	172	2	.	.	PUNCT
eurjchem-1125	173	1	synthesis	synthesis	NOUN
eurjchem-1125	173	2	of	of	ADP
eurjchem-1125	173	3	ethyl	ethyl	PROPN
eurjchem-1125	173	4	2‐(2‐cyano‐3,3‐bis(2‐ethoxy‐2‐oxo	2‐(2‐cyano‐3,3‐bis(2‐ethoxy‐2‐oxo	NUM
eurjchem-1125	173	5	ethylthio)acrylamido)‐4,5,6,7‐tetrahydrobenzo[b]thiophene	ethylthio)acrylamido)‐4,5,6,7‐tetrahydrobenzo[b]thiophene	PROPN
eurjchem-1125	173	6	‐3‐carboxylate	‐3‐carboxylate	NOUN
eurjchem-1125	173	7	(	(	PUNCT
eurjchem-1125	173	8	16	16	NUM
eurjchem-1125	173	9	)	)	PUNCT
eurjchem-1125	173	10	to	to	ADP
eurjchem-1125	173	11	a	a	DET
eurjchem-1125	173	12	cold	cold	ADJ
eurjchem-1125	173	13	suspension	suspension	NOUN
eurjchem-1125	173	14	of	of	ADP
eurjchem-1125	173	15	koh	koh	PROPN
eurjchem-1125	173	16	(	(	PUNCT
eurjchem-1125	173	17	1.16	1.16	NUM
eurjchem-1125	173	18	g	g	NOUN
eurjchem-1125	173	19	,	,	PUNCT
eurjchem-1125	173	20	20	20	NUM
eurjchem-1125	173	21	mmole	mmole	NOUN
eurjchem-1125	173	22	)	)	PUNCT
eurjchem-1125	173	23	in	in	ADP
eurjchem-1125	173	24	dry	dry	ADJ
eurjchem-1125	173	25	dimethylformamide	dimethylformamide	NOUN
eurjchem-1125	173	26	(	(	PUNCT
eurjchem-1125	173	27	25	25	NUM
eurjchem-1125	173	28	ml	ml	NOUN
eurjchem-1125	173	29	)	)	PUNCT
eurjchem-1125	173	30	were	be	AUX
eurjchem-1125	173	31	added	add	VERB
eurjchem-1125	173	32	the	the	DET
eurjchem-1125	173	33	nitrile	nitrile	ADJ
eurjchem-1125	173	34	derivative	derivative	ADJ
eurjchem-1125	173	35	3	3	NUM
eurjchem-1125	173	36	(	(	PUNCT
eurjchem-1125	173	37	1.45	1.45	NUM
eurjchem-1125	173	38	g	g	NOUN
eurjchem-1125	173	39	,	,	PUNCT
eurjchem-1125	173	40	5	5	NUM
eurjchem-1125	173	41	mmole	mmole	NOUN
eurjchem-1125	173	42	)	)	PUNCT
eurjchem-1125	173	43	subsequently	subsequently	ADV
eurjchem-1125	173	44	carbon	carbon	VERB
eurjchem-1125	173	45	disulphide	disulphide	ADV
eurjchem-1125	173	46	(	(	PUNCT
eurjchem-1125	173	47	1.14	1.14	NUM
eurjchem-1125	173	48	g	g	NOUN
eurjchem-1125	173	49	,	,	PUNCT
eurjchem-1125	173	50	15	15	NUM
eurjchem-1125	173	51	mmol	mmol	NOUN
eurjchem-1125	173	52	)	)	PUNCT
eurjchem-1125	173	53	slowly	slowly	ADV
eurjchem-1125	173	54	dropwise	dropwise	NOUN
eurjchem-1125	173	55	under	under	ADP
eurjchem-1125	173	56	stirring	stir	VERB
eurjchem-1125	173	57	over	over	ADP
eurjchem-1125	173	58	a	a	DET
eurjchem-1125	173	59	period	period	NOUN
eurjchem-1125	173	60	of	of	ADP
eurjchem-1125	173	61	15	15	NUM
eurjchem-1125	173	62	min	min	NOUN
eurjchem-1125	173	63	.	.	PROPN
eurjchem-1125	174	1	while	while	SCONJ
eurjchem-1125	174	2	the	the	DET
eurjchem-1125	174	3	temperature	temperature	NOUN
eurjchem-1125	174	4	of	of	ADP
eurjchem-1125	174	5	the	the	DET
eurjchem-1125	174	6	mixture	mixture	NOUN
eurjchem-1125	174	7	was	be	AUX
eurjchem-1125	174	8	maintained	maintain	VERB
eurjchem-1125	174	9	at	at	ADP
eurjchem-1125	174	10	5‐10	5‐10	NUM
eurjchem-1125	174	11	°	°	NOUN
eurjchem-1125	174	12	c	c	NOUN
eurjchem-1125	174	13	.	.	PUNCT
eurjchem-1125	175	1	the	the	DET
eurjchem-1125	175	2	mixture	mixture	NOUN
eurjchem-1125	175	3	was	be	AUX
eurjchem-1125	175	4	stirred	stir	VERB
eurjchem-1125	175	5	at	at	ADP
eurjchem-1125	175	6	room	room	NOUN
eurjchem-1125	175	7	temperature	temperature	NOUN
eurjchem-1125	175	8	for	for	ADP
eurjchem-1125	175	9	12	12	NUM
eurjchem-1125	175	10	h.	h.	NOUN
eurjchem-1125	175	11	then	then	ADV
eurjchem-1125	175	12	cooled	cool	VERB
eurjchem-1125	175	13	again	again	ADV
eurjchem-1125	175	14	at	at	ADP
eurjchem-1125	175	15	0	0	NUM
eurjchem-1125	175	16	°	°	ADP
eurjchem-1125	175	17	c	c	PROPN
eurjchem-1125	175	18	,	,	PUNCT
eurjchem-1125	175	19	ethyl	ethyl	PROPN
eurjchem-1125	175	20	bromoacetate	bromoacetate	NOUN
eurjchem-1125	175	21	(	(	PUNCT
eurjchem-1125	175	22	1.67	1.67	NUM
eurjchem-1125	175	23	g	g	NOUN
eurjchem-1125	175	24	,	,	PUNCT
eurjchem-1125	175	25	10	10	NUM
eurjchem-1125	175	26	mmol	mmol	NOUN
eurjchem-1125	175	27	)	)	PUNCT
eurjchem-1125	175	28	was	be	AUX
eurjchem-1125	175	29	added	add	VERB
eurjchem-1125	175	30	dropwise	dropwise	NOUN
eurjchem-1125	175	31	over	over	ADP
eurjchem-1125	175	32	a	a	DET
eurjchem-1125	175	33	period	period	NOUN
eurjchem-1125	175	34	of	of	ADP
eurjchem-1125	175	35	10	10	NUM
eurjchem-1125	175	36	min	min	NOUN
eurjchem-1125	175	37	and	and	CCONJ
eurjchem-1125	175	38	left	leave	VERB
eurjchem-1125	175	39	to	to	PART
eurjchem-1125	175	40	stand	stand	VERB
eurjchem-1125	175	41	at	at	ADP
eurjchem-1125	175	42	room	room	NOUN
eurjchem-1125	175	43	temperature	temperature	NOUN
eurjchem-1125	175	44	for	for	ADP
eurjchem-1125	175	45	24	24	NUM
eurjchem-1125	175	46	h.	h.	NOUN
eurjchem-1125	175	47	the	the	DET
eurjchem-1125	175	48	mixture	mixture	NOUN
eurjchem-1125	175	49	was	be	AUX
eurjchem-1125	175	50	poured	pour	VERB
eurjchem-1125	175	51	onto	onto	ADP
eurjchem-1125	175	52	ice	ice	NOUN
eurjchem-1125	175	53	cold‐water	cold‐water	NOUN
eurjchem-1125	175	54	.	.	PUNCT
eurjchem-1125	176	1	the	the	DET
eurjchem-1125	176	2	resulting	result	VERB
eurjchem-1125	176	3	precipitate	precipitate	NOUN
eurjchem-1125	176	4	was	be	AUX
eurjchem-1125	176	5	filtered	filter	VERB
eurjchem-1125	176	6	off	off	ADP
eurjchem-1125	176	7	,	,	PUNCT
eurjchem-1125	176	8	dried	dry	VERB
eurjchem-1125	176	9	and	and	CCONJ
eurjchem-1125	176	10	crystallized	crystallize	VERB
eurjchem-1125	176	11	from	from	ADP
eurjchem-1125	176	12	ethanol	ethanol	NOUN
eurjchem-1125	176	13	:	:	PUNCT
eurjchem-1125	176	14	dmf	dmf	PROPN
eurjchem-1125	176	15	(	(	PUNCT
eurjchem-1125	176	16	1:5	1:5	NUM
eurjchem-1125	176	17	,	,	PUNCT
eurjchem-1125	176	18	v	v	NOUN
eurjchem-1125	176	19	:	:	PUNCT
eurjchem-1125	176	20	v	v	NOUN
eurjchem-1125	176	21	)	)	PUNCT
eurjchem-1125	176	22	mixture	mixture	NOUN
eurjchem-1125	176	23	to	to	PART
eurjchem-1125	176	24	give	give	VERB
eurjchem-1125	176	25	compound	compound	NOUN
eurjchem-1125	176	26	16	16	NUM
eurjchem-1125	176	27	(	(	PUNCT
eurjchem-1125	176	28	scheme	scheme	NOUN
eurjchem-1125	176	29	4	4	NUM
eurjchem-1125	176	30	)	)	PUNCT
eurjchem-1125	176	31	.	.	PUNCT
eurjchem-1125	177	1	color	color	NOUN
eurjchem-1125	177	2	:	:	PUNCT
eurjchem-1125	177	3	yellow	yellow	ADJ
eurjchem-1125	177	4	sheet	sheet	NOUN
eurjchem-1125	177	5	crystals	crystal	NOUN
eurjchem-1125	177	6	.	.	PUNCT
eurjchem-1125	178	1	yield	yield	NOUN
eurjchem-1125	178	2	:	:	PUNCT
eurjchem-1125	178	3	2.19	2.19	NUM
eurjchem-1125	178	4	g	g	NOUN
eurjchem-1125	178	5	,	,	PUNCT
eurjchem-1125	178	6	81	81	NUM
eurjchem-1125	178	7	%	%	NOUN
eurjchem-1125	178	8	.	.	PUNCT
eurjchem-1125	179	1	m.p	m.p	PROPN
eurjchem-1125	179	2	.	.	PROPN
eurjchem-1125	179	3	:	:	PUNCT
eurjchem-1125	179	4	178	178	NUM
eurjchem-1125	179	5	°	°	SYM
eurjchem-1125	179	6	c	c	X
eurjchem-1125	179	7	.	.	PUNCT
eurjchem-1125	180	1	ft‐ir	ft‐ir	NOUN
eurjchem-1125	180	2	(	(	PUNCT
eurjchem-1125	180	3	kbr	kbr	PROPN
eurjchem-1125	180	4	,	,	PUNCT
eurjchem-1125	180	5	ν	ν	PROPN
eurjchem-1125	180	6	,	,	PUNCT
eurjchem-1125	180	7	cm‐1	cm‐1	PROPN
eurjchem-1125	180	8	):	):	PUNCT
eurjchem-1125	180	9	3140	3140	NUM
eurjchem-1125	180	10	(	(	PUNCT
eurjchem-1125	180	11	nh	nh	NOUN
eurjchem-1125	180	12	)	)	PUNCT
eurjchem-1125	180	13	,	,	PUNCT
eurjchem-1125	180	14	2170	2170	NUM
eurjchem-1125	180	15	(	(	PUNCT
eurjchem-1125	180	16	cn	cn	PROPN
eurjchem-1125	180	17	)	)	PUNCT
eurjchem-1125	180	18	,	,	PUNCT
eurjchem-1125	180	19	1729	1729	NUM
eurjchem-1125	180	20	,	,	PUNCT
eurjchem-1125	180	21	1677	1677	NUM
eurjchem-1125	180	22	,	,	PUNCT
eurjchem-1125	180	23	1621	1621	NUM
eurjchem-1125	180	24	(	(	PUNCT
eurjchem-1125	180	25	c	c	NOUN
eurjchem-1125	180	26	=	=	NOUN
eurjchem-1125	180	27	o	o	NOUN
eurjchem-1125	180	28	)	)	PUNCT
eurjchem-1125	180	29	.	.	PUNCT
eurjchem-1125	181	1	1h	1h	NUM
eurjchem-1125	181	2	nmr	nmr	NOUN
eurjchem-1125	181	3	(	(	PUNCT
eurjchem-1125	181	4	400	400	NUM
eurjchem-1125	181	5	mhz	mhz	NOUN
eurjchem-1125	181	6	,	,	PUNCT
eurjchem-1125	181	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	181	8	,	,	PUNCT
eurjchem-1125	181	9	δ	δ	PROPN
eurjchem-1125	181	10	,	,	PUNCT
eurjchem-1125	181	11	ppm	ppm	NUM
eurjchem-1125	181	12	):	):	PUNCT
eurjchem-1125	181	13	1.14	1.14	NUM
eurjchem-1125	181	14	(	(	PUNCT
eurjchem-1125	181	15	t	t	PROPN
eurjchem-1125	181	16	,	,	PUNCT
eurjchem-1125	181	17	3h	3h	NUM
eurjchem-1125	181	18	,	,	PUNCT
eurjchem-1125	181	19	j	j	PROPN
eurjchem-1125	181	20	=	=	SYM
eurjchem-1125	181	21	6.8	6.8	NUM
eurjchem-1125	181	22	hz	hz	NOUN
eurjchem-1125	181	23	,	,	PUNCT
eurjchem-1125	181	24	ch3	ch3	PROPN
eurjchem-1125	181	25	)	)	PUNCT
eurjchem-1125	181	26	,	,	PUNCT
eurjchem-1125	181	27	1.25	1.25	NUM
eurjchem-1125	181	28	(	(	PUNCT
eurjchem-1125	181	29	t	t	PROPN
eurjchem-1125	181	30	,	,	PUNCT
eurjchem-1125	181	31	3h	3h	NUM
eurjchem-1125	181	32	,	,	PUNCT
eurjchem-1125	181	33	j	j	PROPN
eurjchem-1125	181	34	=	=	SYM
eurjchem-1125	181	35	6.8	6.8	NUM
eurjchem-1125	181	36	hz	hz	NOUN
eurjchem-1125	181	37	,	,	PUNCT
eurjchem-1125	181	38	ch3	ch3	PROPN
eurjchem-1125	181	39	)	)	PUNCT
eurjchem-1125	181	40	,	,	PUNCT
eurjchem-1125	181	41	1.28	1.28	NUM
eurjchem-1125	181	42	(	(	PUNCT
eurjchem-1125	181	43	t	t	PROPN
eurjchem-1125	181	44	,	,	PUNCT
eurjchem-1125	181	45	3h	3h	NUM
eurjchem-1125	181	46	,	,	PUNCT
eurjchem-1125	181	47	j	j	PROPN
eurjchem-1125	181	48	=	=	SYM
eurjchem-1125	181	49	6.8	6.8	NUM
eurjchem-1125	181	50	hz	hz	NOUN
eurjchem-1125	181	51	,	,	PUNCT
eurjchem-1125	181	52	ch3	ch3	PROPN
eurjchem-1125	181	53	)	)	PUNCT
eurjchem-1125	181	54	,	,	PUNCT
eurjchem-1125	181	55	1.75‐1.78	1.75‐1.78	NUM
eurjchem-1125	181	56	(	(	PUNCT
eurjchem-1125	181	57	m	m	PROPN
eurjchem-1125	181	58	,	,	PUNCT
eurjchem-1125	181	59	4h	4h	NOUN
eurjchem-1125	181	60	,	,	PUNCT
eurjchem-1125	181	61	c5‐2h	c5‐2h	PROPN
eurjchem-1125	181	62	,	,	PUNCT
eurjchem-1125	181	63	c6‐2h	c6‐2h	NOUN
eurjchem-1125	181	64	,	,	PUNCT
eurjchem-1125	181	65	cyclohexane	cyclohexane	NOUN
eurjchem-1125	181	66	skeleton	skeleton	NOUN
eurjchem-1125	181	67	)	)	PUNCT
eurjchem-1125	181	68	,	,	PUNCT
eurjchem-1125	181	69	2.65‐2.79	2.65‐2.79	NUM
eurjchem-1125	181	70	(	(	PUNCT
eurjchem-1125	181	71	m	m	PROPN
eurjchem-1125	181	72	,	,	PUNCT
eurjchem-1125	181	73	4h	4h	NUM
eurjchem-1125	181	74	,	,	PUNCT
eurjchem-1125	181	75	c4‐2h	c4‐2h	PROPN
eurjchem-1125	181	76	,	,	PUNCT
eurjchem-1125	181	77	c7‐2h	c7‐2h	PROPN
eurjchem-1125	181	78	,	,	PUNCT
eurjchem-1125	181	79	cyclohexane	cyclohexane	NOUN
eurjchem-1125	181	80	skeleton	skeleton	NOUN
eurjchem-1125	181	81	)	)	PUNCT
eurjchem-1125	181	82	,	,	PUNCT
eurjchem-1125	181	83	3.17	3.17	NUM
eurjchem-1125	181	84	(	(	PUNCT
eurjchem-1125	181	85	br	br	PROPN
eurjchem-1125	181	86	,	,	PUNCT
eurjchem-1125	181	87	4h	4h	NOUN
eurjchem-1125	181	88	,	,	PUNCT
eurjchem-1125	181	89	2ch2	2ch2	NUM
eurjchem-1125	181	90	)	)	PUNCT
eurjchem-1125	181	91	,	,	PUNCT
eurjchem-1125	181	92	4.07	4.07	NUM
eurjchem-1125	181	93	(	(	PUNCT
eurjchem-1125	181	94	q	q	NOUN
eurjchem-1125	181	95	,	,	PUNCT
eurjchem-1125	181	96	2h	2h	NUM
eurjchem-1125	181	97	,	,	PUNCT
eurjchem-1125	181	98	j	j	PROPN
eurjchem-1125	181	99	=	=	SYM
eurjchem-1125	181	100	6.8	6.8	NUM
eurjchem-1125	181	101	hz	hz	NOUN
eurjchem-1125	181	102	,	,	PUNCT
eurjchem-1125	181	103	ch2o	ch2o	NOUN
eurjchem-1125	181	104	)	)	PUNCT
eurjchem-1125	181	105	,	,	PUNCT
eurjchem-1125	181	106	4.18	4.18	NUM
eurjchem-1125	181	107	(	(	PUNCT
eurjchem-1125	181	108	q	q	NOUN
eurjchem-1125	181	109	,	,	PUNCT
eurjchem-1125	181	110	2h	2h	NUM
eurjchem-1125	181	111	,	,	PUNCT
eurjchem-1125	181	112	j	j	PROPN
eurjchem-1125	181	113	=	=	SYM
eurjchem-1125	181	114	6.8	6.8	NUM
eurjchem-1125	181	115	hz	hz	NOUN
eurjchem-1125	181	116	,	,	PUNCT
eurjchem-1125	181	117	ch2o	ch2o	NOUN
eurjchem-1125	181	118	)	)	PUNCT
eurjchem-1125	181	119	,	,	PUNCT
eurjchem-1125	181	120	4.31	4.31	NUM
eurjchem-1125	181	121	(	(	PUNCT
eurjchem-1125	181	122	q	q	NOUN
eurjchem-1125	181	123	,	,	PUNCT
eurjchem-1125	181	124	2h	2h	NUM
eurjchem-1125	181	125	,	,	PUNCT
eurjchem-1125	181	126	j	j	PROPN
eurjchem-1125	181	127	=	=	SYM
eurjchem-1125	181	128	6.8	6.8	NUM
eurjchem-1125	181	129	hz	hz	NOUN
eurjchem-1125	181	130	,	,	PUNCT
eurjchem-1125	181	131	ch2o	ch2o	NOUN
eurjchem-1125	181	132	)	)	PUNCT
eurjchem-1125	181	133	,	,	PUNCT
eurjchem-1125	181	134	12.66	12.66	NUM
eurjchem-1125	181	135	(	(	PUNCT
eurjchem-1125	181	136	s	s	PROPN
eurjchem-1125	181	137	,	,	PUNCT
eurjchem-1125	181	138	1h	1h	NUM
eurjchem-1125	181	139	,	,	PUNCT
eurjchem-1125	181	140	nh‐co	nh‐co	NUM
eurjchem-1125	181	141	)	)	PUNCT
eurjchem-1125	181	142	.	.	PUNCT
eurjchem-1125	182	1	13c	13c	NOUN
eurjchem-1125	182	2	nmr	nmr	NOUN
eurjchem-1125	182	3	(	(	PUNCT
eurjchem-1125	182	4	100	100	NUM
eurjchem-1125	182	5	mhz	mhz	NOUN
eurjchem-1125	182	6	,	,	PUNCT
eurjchem-1125	182	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	182	8	,	,	PUNCT
eurjchem-1125	182	9	δ	δ	PROPN
eurjchem-1125	182	10	,	,	PUNCT
eurjchem-1125	182	11	ppm	ppm	NUM
eurjchem-1125	182	12	):	):	PUNCT
eurjchem-1125	182	13	169.4	169.4	NUM
eurjchem-1125	182	14	,	,	PUNCT
eurjchem-1125	182	15	166.5	166.5	NUM
eurjchem-1125	182	16	,	,	PUNCT
eurjchem-1125	182	17	166.4	166.4	NUM
eurjchem-1125	182	18	,	,	PUNCT
eurjchem-1125	182	19	163.9	163.9	NUM
eurjchem-1125	182	20	,	,	PUNCT
eurjchem-1125	182	21	145.9	145.9	NUM
eurjchem-1125	182	22	,	,	PUNCT
eurjchem-1125	182	23	143.1	143.1	NUM
eurjchem-1125	182	24	,	,	PUNCT
eurjchem-1125	182	25	132.7	132.7	NUM
eurjchem-1125	182	26	,	,	PUNCT
eurjchem-1125	182	27	127.9	127.9	NUM
eurjchem-1125	182	28	,	,	PUNCT
eurjchem-1125	182	29	115.2	115.2	NUM
eurjchem-1125	182	30	,	,	PUNCT
eurjchem-1125	182	31	61.4	61.4	NUM
eurjchem-1125	182	32	,	,	PUNCT
eurjchem-1125	182	33	61.0	61.0	NUM
eurjchem-1125	182	34	,	,	PUNCT
eurjchem-1125	182	35	60.2	60.2	NUM
eurjchem-1125	182	36	,	,	PUNCT
eurjchem-1125	182	37	37.1	37.1	NUM
eurjchem-1125	182	38	,	,	PUNCT
eurjchem-1125	182	39	36.7	36.7	NUM
eurjchem-1125	182	40	,	,	PUNCT
eurjchem-1125	182	41	25.6	25.6	NUM
eurjchem-1125	182	42	,	,	PUNCT
eurjchem-1125	182	43	23.6	23.6	NUM
eurjchem-1125	182	44	,	,	PUNCT
eurjchem-1125	182	45	22.2	22.2	NUM
eurjchem-1125	182	46	,	,	PUNCT
eurjchem-1125	182	47	22.1	22.1	NUM
eurjchem-1125	182	48	,	,	PUNCT
eurjchem-1125	182	49	13.8	13.8	NUM
eurjchem-1125	182	50	,	,	PUNCT
eurjchem-1125	182	51	and	and	CCONJ
eurjchem-1125	182	52	13.6	13.6	NUM
eurjchem-1125	182	53	.	.	PUNCT
eurjchem-1125	182	54	ei‐ms	ei‐ms	PROPN
eurjchem-1125	182	55	(	(	PUNCT
eurjchem-1125	182	56	m	m	NOUN
eurjchem-1125	182	57	/	/	SYM
eurjchem-1125	182	58	z	z	NOUN
eurjchem-1125	182	59	(	(	PUNCT
eurjchem-1125	182	60	%	%	NOUN
eurjchem-1125	182	61	)	)	PUNCT
eurjchem-1125	182	62	):	):	PUNCT
eurjchem-1125	182	63	540	540	NUM
eurjchem-1125	182	64	(	(	PUNCT
eurjchem-1125	182	65	m+	m+	NUM
eurjchem-1125	182	66	,	,	PUNCT
eurjchem-1125	182	67	0.8	0.8	NUM
eurjchem-1125	182	68	)	)	PUNCT
eurjchem-1125	182	69	,	,	PUNCT
eurjchem-1125	182	70	529	529	NUM
eurjchem-1125	182	71	(	(	PUNCT
eurjchem-1125	182	72	3.9	3.9	NUM
eurjchem-1125	182	73	)	)	PUNCT
eurjchem-1125	182	74	,	,	PUNCT
eurjchem-1125	182	75	424	424	NUM
eurjchem-1125	182	76	(	(	PUNCT
eurjchem-1125	182	77	35.3	35.3	NUM
eurjchem-1125	182	78	)	)	PUNCT
eurjchem-1125	182	79	,	,	PUNCT
eurjchem-1125	182	80	385	385	NUM
eurjchem-1125	182	81	(	(	PUNCT
eurjchem-1125	182	82	2.8	2.8	NUM
eurjchem-1125	182	83	)	)	PUNCT
eurjchem-1125	182	84	,	,	PUNCT
eurjchem-1125	182	85	366	366	NUM
eurjchem-1125	182	86	(	(	PUNCT
eurjchem-1125	182	87	5.2	5.2	NUM
eurjchem-1125	182	88	)	)	PUNCT
eurjchem-1125	182	89	,	,	PUNCT
eurjchem-1125	182	90	338	338	NUM
eurjchem-1125	182	91	(	(	PUNCT
eurjchem-1125	182	92	2.0	2.0	NUM
eurjchem-1125	182	93	)	)	PUNCT
eurjchem-1125	182	94	,	,	PUNCT
eurjchem-1125	182	95	224	224	NUM
eurjchem-1125	182	96	(	(	PUNCT
eurjchem-1125	182	97	20.6	20.6	NUM
eurjchem-1125	182	98	)	)	PUNCT
eurjchem-1125	182	99	,	,	PUNCT
eurjchem-1125	182	100	205	205	NUM
eurjchem-1125	182	101	(	(	PUNCT
eurjchem-1125	182	102	39.5	39.5	NUM
eurjchem-1125	182	103	)	)	PUNCT
eurjchem-1125	182	104	,	,	PUNCT
eurjchem-1125	182	105	177	177	NUM
eurjchem-1125	182	106	(	(	PUNCT
eurjchem-1125	182	107	76.4	76.4	NUM
eurjchem-1125	182	108	)	)	PUNCT
eurjchem-1125	182	109	,	,	PUNCT
eurjchem-1125	182	110	150	150	NUM
eurjchem-1125	182	111	(	(	PUNCT
eurjchem-1125	182	112	69.0	69.0	NUM
eurjchem-1125	182	113	)	)	PUNCT
eurjchem-1125	182	114	,	,	PUNCT
eurjchem-1125	182	115	134	134	NUM
eurjchem-1125	182	116	(	(	PUNCT
eurjchem-1125	182	117	63.9	63.9	NUM
eurjchem-1125	182	118	)	)	PUNCT
eurjchem-1125	182	119	,	,	PUNCT
eurjchem-1125	182	120	119	119	NUM
eurjchem-1125	182	121	(	(	PUNCT
eurjchem-1125	182	122	52.1	52.1	NUM
eurjchem-1125	182	123	)	)	PUNCT
eurjchem-1125	182	124	,	,	PUNCT
eurjchem-1125	182	125	108	108	NUM
eurjchem-1125	182	126	(	(	PUNCT
eurjchem-1125	182	127	81.9	81.9	NUM
eurjchem-1125	182	128	)	)	PUNCT
eurjchem-1125	182	129	,	,	PUNCT
eurjchem-1125	182	130	101	101	NUM
eurjchem-1125	182	131	(	(	PUNCT
eurjchem-1125	182	132	69.9	69.9	NUM
eurjchem-1125	182	133	)	)	PUNCT
eurjchem-1125	182	134	,	,	PUNCT
eurjchem-1125	182	135	83(76.3	83(76.3	NOUN
eurjchem-1125	182	136	)	)	PUNCT
eurjchem-1125	182	137	,	,	PUNCT
eurjchem-1125	182	138	76	76	NUM
eurjchem-1125	182	139	(	(	PUNCT
eurjchem-1125	182	140	100	100	NUM
eurjchem-1125	182	141	)	)	PUNCT
eurjchem-1125	182	142	,	,	PUNCT
eurjchem-1125	182	143	63	63	NUM
eurjchem-1125	182	144	(	(	PUNCT
eurjchem-1125	182	145	87.3	87.3	NUM
eurjchem-1125	182	146	)	)	PUNCT
eurjchem-1125	182	147	.	.	PUNCT
eurjchem-1125	183	1	anal	anal	PROPN
eurjchem-1125	183	2	.	.	PUNCT
eurjchem-1125	183	3	calcd	calcd	NOUN
eurjchem-1125	183	4	.	.	PUNCT
eurjchem-1125	184	1	for	for	ADP
eurjchem-1125	184	2	c23h29n2o7s3	c23h29n2o7s3	ADJ
eurjchem-1125	184	3	:	:	PUNCT
eurjchem-1125	184	4	c	c	X
eurjchem-1125	184	5	,	,	PUNCT
eurjchem-1125	184	6	51.09	51.09	NUM
eurjchem-1125	184	7	;	;	PUNCT
eurjchem-1125	184	8	h	h	X
eurjchem-1125	184	9	,	,	PUNCT
eurjchem-1125	184	10	5.22	5.22	NUM
eurjchem-1125	184	11	;	;	PUNCT
eurjchem-1125	184	12	n	n	CCONJ
eurjchem-1125	184	13	,	,	PUNCT
eurjchem-1125	184	14	5.18	5.18	NUM
eurjchem-1125	184	15	.	.	PUNCT
eurjchem-1125	184	16	found	find	VERB
eurjchem-1125	184	17	:	:	PUNCT
eurjchem-1125	185	1	51.15	51.15	NUM
eurjchem-1125	185	2	;	;	PUNCT
eurjchem-1125	185	3	h	h	NOUN
eurjchem-1125	185	4	,	,	PUNCT
eurjchem-1125	185	5	5.18	5.18	NUM
eurjchem-1125	185	6	;	;	PUNCT
eurjchem-1125	185	7	n	n	CCONJ
eurjchem-1125	185	8	,	,	PUNCT
eurjchem-1125	185	9	5.19	5.19	NUM
eurjchem-1125	185	10	%	%	NOUN
eurjchem-1125	185	11	.	.	PUNCT
eurjchem-1125	186	1	2.2.8	2.2.8	X
eurjchem-1125	186	2	.	.	PUNCT
eurjchem-1125	187	1	synthesis	synthesis	NOUN
eurjchem-1125	187	2	of	of	ADP
eurjchem-1125	187	3	ethyl	ethyl	PROPN
eurjchem-1125	187	4	2‐(4‐amino‐2‐(2‐ethoxy‐2‐oxoethyl	2‐(4‐amino‐2‐(2‐ethoxy‐2‐oxoethyl	NUM
eurjchem-1125	187	5	thio)‐5‐(ethoxycarbonyl	thio)‐5‐(ethoxycarbonyl	PROPN
eurjchem-1125	187	6	)	)	PUNCT
eurjchem-1125	187	7	thiophene‐3‐carboxamido)‐4,5,6,7‐	thiophene‐3‐carboxamido)‐4,5,6,7‐	NOUN
eurjchem-1125	187	8	tetrahydrobenzo[b]thiophene‐3‐carboxylate	tetrahydrobenzo[b]thiophene‐3‐carboxylate	NOUN
eurjchem-1125	187	9	(	(	PUNCT
eurjchem-1125	187	10	17	17	NUM
eurjchem-1125	187	11	)	)	PUNCT
eurjchem-1125	187	12	a	a	DET
eurjchem-1125	187	13	mixture	mixture	NOUN
eurjchem-1125	187	14	of	of	ADP
eurjchem-1125	187	15	compound	compound	NOUN
eurjchem-1125	187	16	16	16	NUM
eurjchem-1125	187	17	(	(	PUNCT
eurjchem-1125	187	18	0.54	0.54	NUM
eurjchem-1125	187	19	g	g	NOUN
eurjchem-1125	187	20	,	,	PUNCT
eurjchem-1125	187	21	1.0	1.0	NUM
eurjchem-1125	187	22	mmol	mmol	NOUN
eurjchem-1125	187	23	)	)	PUNCT
eurjchem-1125	187	24	and	and	CCONJ
eurjchem-1125	187	25	tea	tea	NOUN
eurjchem-1125	187	26	(	(	PUNCT
eurjchem-1125	187	27	0.2	0.2	NUM
eurjchem-1125	187	28	ml	ml	NOUN
eurjchem-1125	187	29	)	)	PUNCT
eurjchem-1125	187	30	in	in	ADP
eurjchem-1125	187	31	dmf	dmf	PROPN
eurjchem-1125	187	32	(	(	PUNCT
eurjchem-1125	187	33	15	15	NUM
eurjchem-1125	187	34	ml	ml	NOUN
eurjchem-1125	187	35	)	)	PUNCT
eurjchem-1125	187	36	was	be	AUX
eurjchem-1125	187	37	stirred	stir	VERB
eurjchem-1125	187	38	at	at	ADP
eurjchem-1125	187	39	140	140	NUM
eurjchem-1125	187	40	°	°	NOUN
eurjchem-1125	187	41	c	c	NOUN
eurjchem-1125	187	42	.	.	PUNCT
eurjchem-1125	188	1	648	648	NUM
eurjchem-1125	188	2	gouda	gouda	NOUN
eurjchem-1125	188	3	and	and	CCONJ
eurjchem-1125	188	4	el‐bialy	el‐bialy	PROPN
eurjchem-1125	188	5	/	/	SYM
eurjchem-1125	188	6	european	european	PROPN
eurjchem-1125	188	7	journal	journal	PROPN
eurjchem-1125	188	8	of	of	ADP
eurjchem-1125	188	9	chemistry	chemistry	NOUN
eurjchem-1125	188	10	5	5	NUM
eurjchem-1125	188	11	(	(	PUNCT
eurjchem-1125	188	12	4	4	NUM
eurjchem-1125	188	13	)	)	PUNCT
eurjchem-1125	188	14	(	(	PUNCT
eurjchem-1125	188	15	2014	2014	NUM
eurjchem-1125	188	16	)	)	PUNCT
eurjchem-1125	189	1	644‐651	644‐651	NUM
eurjchem-1125	189	2	scheme	scheme	NOUN
eurjchem-1125	189	3	4	4	NUM
eurjchem-1125	189	4	the	the	DET
eurjchem-1125	189	5	mixture	mixture	NOUN
eurjchem-1125	189	6	was	be	AUX
eurjchem-1125	189	7	cooled	cool	VERB
eurjchem-1125	189	8	,	,	PUNCT
eurjchem-1125	189	9	poured	pour	VERB
eurjchem-1125	189	10	into	into	ADP
eurjchem-1125	189	11	cooled	cool	VERB
eurjchem-1125	189	12	water	water	NOUN
eurjchem-1125	189	13	,	,	PUNCT
eurjchem-1125	189	14	the	the	DET
eurjchem-1125	189	15	separated	separate	VERB
eurjchem-1125	189	16	crystals	crystal	NOUN
eurjchem-1125	189	17	was	be	AUX
eurjchem-1125	189	18	filtered	filter	VERB
eurjchem-1125	189	19	,	,	PUNCT
eurjchem-1125	189	20	dried	dry	VERB
eurjchem-1125	189	21	and	and	CCONJ
eurjchem-1125	189	22	crystallize	crystallize	VERB
eurjchem-1125	189	23	from	from	ADP
eurjchem-1125	189	24	dmf	dmf	PROPN
eurjchem-1125	189	25	:	:	PUNCT
eurjchem-1125	189	26	etoh	etoh	PROPN
eurjchem-1125	189	27	(	(	PUNCT
eurjchem-1125	189	28	1:2	1:2	NUM
eurjchem-1125	189	29	,	,	PUNCT
eurjchem-1125	189	30	v	v	NOUN
eurjchem-1125	189	31	:	:	PUNCT
eurjchem-1125	189	32	v	v	NOUN
eurjchem-1125	189	33	)	)	PUNCT
eurjchem-1125	189	34	mixture	mixture	NOUN
eurjchem-1125	189	35	to	to	PART
eurjchem-1125	189	36	give	give	VERB
eurjchem-1125	189	37	compound	compound	NOUN
eurjchem-1125	189	38	17	17	NUM
eurjchem-1125	189	39	(	(	PUNCT
eurjchem-1125	189	40	scheme	scheme	NOUN
eurjchem-1125	189	41	4	4	NUM
eurjchem-1125	189	42	)	)	PUNCT
eurjchem-1125	189	43	.	.	PUNCT
eurjchem-1125	190	1	color	color	NOUN
eurjchem-1125	190	2	:	:	PUNCT
eurjchem-1125	190	3	brown	brown	ADJ
eurjchem-1125	190	4	powder	powder	NOUN
eurjchem-1125	190	5	.	.	PUNCT
eurjchem-1125	191	1	yield	yield	NOUN
eurjchem-1125	191	2	:	:	PUNCT
eurjchem-1125	191	3	0.36	0.36	NUM
eurjchem-1125	191	4	g	g	NOUN
eurjchem-1125	191	5	,	,	PUNCT
eurjchem-1125	191	6	66	66	NUM
eurjchem-1125	191	7	%	%	NOUN
eurjchem-1125	191	8	.	.	PUNCT
eurjchem-1125	192	1	m.p	m.p	PROPN
eurjchem-1125	192	2	.	.	PROPN
eurjchem-1125	192	3	:	:	PUNCT
eurjchem-1125	193	1	192	192	NUM
eurjchem-1125	193	2	°	°	SYM
eurjchem-1125	193	3	c	c	X
eurjchem-1125	193	4	.	.	PUNCT
eurjchem-1125	194	1	ft‐ir	ft‐ir	NOUN
eurjchem-1125	194	2	(	(	PUNCT
eurjchem-1125	194	3	kbr	kbr	PROPN
eurjchem-1125	194	4	,	,	PUNCT
eurjchem-1125	194	5	ν	ν	PROPN
eurjchem-1125	194	6	,	,	PUNCT
eurjchem-1125	194	7	cm‐1	cm‐1	PROPN
eurjchem-1125	194	8	):	):	PUNCT
eurjchem-1125	194	9	3411	3411	NUM
eurjchem-1125	194	10	,	,	PUNCT
eurjchem-1125	194	11	3280	3280	NUM
eurjchem-1125	194	12	,	,	PUNCT
eurjchem-1125	194	13	3261	3261	NUM
eurjchem-1125	194	14	(	(	PUNCT
eurjchem-1125	194	15	nh	nh	PROPN
eurjchem-1125	194	16	,	,	PUNCT
eurjchem-1125	194	17	nh2	nh2	PROPN
eurjchem-1125	194	18	)	)	PUNCT
eurjchem-1125	194	19	,	,	PUNCT
eurjchem-1125	194	20	1714	1714	NUM
eurjchem-1125	194	21	,	,	PUNCT
eurjchem-1125	194	22	1677	1677	NUM
eurjchem-1125	194	23	,	,	PUNCT
eurjchem-1125	194	24	1614	1614	NUM
eurjchem-1125	194	25	(	(	PUNCT
eurjchem-1125	194	26	c	c	NOUN
eurjchem-1125	194	27	=	=	NOUN
eurjchem-1125	194	28	o	o	NOUN
eurjchem-1125	194	29	)	)	PUNCT
eurjchem-1125	194	30	.	.	PUNCT
eurjchem-1125	195	1	1h	1h	NUM
eurjchem-1125	195	2	nmr	nmr	NOUN
eurjchem-1125	195	3	(	(	PUNCT
eurjchem-1125	195	4	400	400	NUM
eurjchem-1125	195	5	mhz	mhz	NOUN
eurjchem-1125	195	6	,	,	PUNCT
eurjchem-1125	195	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	195	8	,	,	PUNCT
eurjchem-1125	195	9	δ	δ	PROPN
eurjchem-1125	195	10	,	,	PUNCT
eurjchem-1125	195	11	ppm	ppm	NUM
eurjchem-1125	195	12	):	):	PUNCT
eurjchem-1125	195	13	1.21‐1.28	1.21‐1.28	NUM
eurjchem-1125	195	14	(	(	PUNCT
eurjchem-1125	195	15	m	m	PROPN
eurjchem-1125	195	16	,	,	PUNCT
eurjchem-1125	195	17	9h	9h	NOUN
eurjchem-1125	195	18	,	,	PUNCT
eurjchem-1125	195	19	3ch3	3ch3	NUM
eurjchem-1125	195	20	)	)	PUNCT
eurjchem-1125	195	21	,	,	PUNCT
eurjchem-1125	195	22	1.74‐1.77	1.74‐1.77	NUM
eurjchem-1125	195	23	(	(	PUNCT
eurjchem-1125	195	24	m	m	PROPN
eurjchem-1125	195	25	,	,	PUNCT
eurjchem-1125	195	26	4h	4h	NOUN
eurjchem-1125	195	27	,	,	PUNCT
eurjchem-1125	195	28	c5‐2h	c5‐2h	PROPN
eurjchem-1125	195	29	,	,	PUNCT
eurjchem-1125	195	30	c6‐2h	c6‐2h	NOUN
eurjchem-1125	195	31	,	,	PUNCT
eurjchem-1125	195	32	cyclohexane	cyclohexane	NOUN
eurjchem-1125	195	33	skeleton	skeleton	NOUN
eurjchem-1125	195	34	)	)	PUNCT
eurjchem-1125	195	35	,	,	PUNCT
eurjchem-1125	195	36	2.65‐2.79	2.65‐2.79	NUM
eurjchem-1125	195	37	(	(	PUNCT
eurjchem-1125	195	38	m	m	PROPN
eurjchem-1125	195	39	,	,	PUNCT
eurjchem-1125	195	40	4h	4h	NUM
eurjchem-1125	195	41	,	,	PUNCT
eurjchem-1125	195	42	c4‐2h	c4‐2h	PROPN
eurjchem-1125	195	43	,	,	PUNCT
eurjchem-1125	195	44	c7‐2h	c7‐2h	PROPN
eurjchem-1125	195	45	,	,	PUNCT
eurjchem-1125	195	46	cyclohexane	cyclohexane	NOUN
eurjchem-1125	195	47	skeleton	skeleton	NOUN
eurjchem-1125	195	48	)	)	PUNCT
eurjchem-1125	195	49	,	,	PUNCT
eurjchem-1125	195	50	3.16	3.16	NUM
eurjchem-1125	195	51	(	(	PUNCT
eurjchem-1125	195	52	s	s	PROPN
eurjchem-1125	195	53	,	,	PUNCT
eurjchem-1125	195	54	2h	2h	NUM
eurjchem-1125	195	55	,	,	PUNCT
eurjchem-1125	195	56	ch2	ch2	PROPN
eurjchem-1125	195	57	)	)	PUNCT
eurjchem-1125	195	58	,	,	PUNCT
eurjchem-1125	195	59	4.26‐4.31	4.26‐4.31	NUM
eurjchem-1125	195	60	(	(	PUNCT
eurjchem-1125	195	61	m	m	PROPN
eurjchem-1125	195	62	,	,	PUNCT
eurjchem-1125	195	63	6h	6h	NUM
eurjchem-1125	195	64	,	,	PUNCT
eurjchem-1125	195	65	j	j	PROPN
eurjchem-1125	195	66	=	=	SYM
eurjchem-1125	195	67	6.8	6.8	NUM
eurjchem-1125	195	68	hz	hz	NOUN
eurjchem-1125	195	69	,	,	PUNCT
eurjchem-1125	195	70	3ch2o	3ch2o	NUM
eurjchem-1125	195	71	)	)	PUNCT
eurjchem-1125	195	72	,	,	PUNCT
eurjchem-1125	195	73	5.08	5.08	NUM
eurjchem-1125	195	74	(	(	PUNCT
eurjchem-1125	195	75	br	br	NOUN
eurjchem-1125	195	76	,	,	PUNCT
eurjchem-1125	195	77	2h	2h	NUM
eurjchem-1125	195	78	,	,	PUNCT
eurjchem-1125	195	79	nh2	nh2	PROPN
eurjchem-1125	195	80	)	)	PUNCT
eurjchem-1125	195	81	,	,	PUNCT
eurjchem-1125	195	82	12.03	12.03	NUM
eurjchem-1125	195	83	(	(	PUNCT
eurjchem-1125	195	84	s	s	PROPN
eurjchem-1125	195	85	,	,	PUNCT
eurjchem-1125	195	86	1h	1h	NUM
eurjchem-1125	195	87	,	,	PUNCT
eurjchem-1125	195	88	nhco	nhco	ADJ
eurjchem-1125	195	89	)	)	PUNCT
eurjchem-1125	195	90	.	.	PUNCT
eurjchem-1125	196	1	ei‐ms	ei‐ms	PROPN
eurjchem-1125	196	2	(	(	PUNCT
eurjchem-1125	196	3	m	m	NOUN
eurjchem-1125	196	4	/	/	SYM
eurjchem-1125	196	5	z	z	NOUN
eurjchem-1125	196	6	(	(	PUNCT
eurjchem-1125	196	7	%	%	NOUN
eurjchem-1125	196	8	)	)	PUNCT
eurjchem-1125	196	9	):	):	PUNCT
eurjchem-1125	196	10	541	541	NUM
eurjchem-1125	196	11	(	(	PUNCT
eurjchem-1125	196	12	m++1	m++1	NOUN
eurjchem-1125	196	13	,	,	PUNCT
eurjchem-1125	196	14	0.2	0.2	NUM
eurjchem-1125	196	15	)	)	PUNCT
eurjchem-1125	196	16	,	,	PUNCT
eurjchem-1125	196	17	525	525	NUM
eurjchem-1125	196	18	(	(	PUNCT
eurjchem-1125	196	19	3.5	3.5	NUM
eurjchem-1125	196	20	)	)	PUNCT
eurjchem-1125	196	21	,	,	PUNCT
eurjchem-1125	196	22	464	464	NUM
eurjchem-1125	196	23	(	(	PUNCT
eurjchem-1125	196	24	1.1	1.1	NUM
eurjchem-1125	196	25	)	)	PUNCT
eurjchem-1125	196	26	,	,	PUNCT
eurjchem-1125	196	27	422	422	NUM
eurjchem-1125	196	28	(	(	PUNCT
eurjchem-1125	196	29	1.9	1.9	NUM
eurjchem-1125	196	30	)	)	PUNCT
eurjchem-1125	196	31	,	,	PUNCT
eurjchem-1125	196	32	390	390	NUM
eurjchem-1125	196	33	(	(	PUNCT
eurjchem-1125	196	34	1.7	1.7	NUM
eurjchem-1125	196	35	)	)	PUNCT
eurjchem-1125	196	36	,	,	PUNCT
eurjchem-1125	196	37	377	377	NUM
eurjchem-1125	196	38	(	(	PUNCT
eurjchem-1125	196	39	35.2	35.2	NUM
eurjchem-1125	196	40	)	)	PUNCT
eurjchem-1125	196	41	,	,	PUNCT
eurjchem-1125	196	42	346	346	NUM
eurjchem-1125	196	43	(	(	PUNCT
eurjchem-1125	196	44	2.6	2.6	NUM
eurjchem-1125	196	45	)	)	PUNCT
eurjchem-1125	196	46	,	,	PUNCT
eurjchem-1125	196	47	238	238	NUM
eurjchem-1125	196	48	(	(	PUNCT
eurjchem-1125	196	49	5.3	5.3	NUM
eurjchem-1125	196	50	)	)	PUNCT
eurjchem-1125	196	51	,	,	PUNCT
eurjchem-1125	196	52	225	225	NUM
eurjchem-1125	196	53	(	(	PUNCT
eurjchem-1125	196	54	30.2	30.2	NUM
eurjchem-1125	196	55	)	)	PUNCT
eurjchem-1125	196	56	,	,	PUNCT
eurjchem-1125	196	57	206	206	NUM
eurjchem-1125	196	58	(	(	PUNCT
eurjchem-1125	196	59	19.3	19.3	NUM
eurjchem-1125	196	60	)	)	PUNCT
eurjchem-1125	196	61	,	,	PUNCT
eurjchem-1125	196	62	177	177	NUM
eurjchem-1125	196	63	(	(	PUNCT
eurjchem-1125	196	64	35.2	35.2	NUM
eurjchem-1125	196	65	)	)	PUNCT
eurjchem-1125	196	66	,	,	PUNCT
eurjchem-1125	196	67	165	165	NUM
eurjchem-1125	196	68	(	(	PUNCT
eurjchem-1125	196	69	10.1	10.1	NUM
eurjchem-1125	196	70	)	)	PUNCT
eurjchem-1125	196	71	,	,	PUNCT
eurjchem-1125	196	72	150	150	NUM
eurjchem-1125	196	73	(	(	PUNCT
eurjchem-1125	196	74	46.5	46.5	NUM
eurjchem-1125	196	75	)	)	PUNCT
eurjchem-1125	196	76	,	,	PUNCT
eurjchem-1125	196	77	120	120	NUM
eurjchem-1125	196	78	(	(	PUNCT
eurjchem-1125	196	79	89.1	89.1	NUM
eurjchem-1125	196	80	)	)	PUNCT
eurjchem-1125	196	81	,	,	PUNCT
eurjchem-1125	196	82	108	108	NUM
eurjchem-1125	196	83	(	(	PUNCT
eurjchem-1125	196	84	95.3	95.3	NUM
eurjchem-1125	196	85	)	)	PUNCT
eurjchem-1125	196	86	,	,	PUNCT
eurjchem-1125	196	87	93	93	NUM
eurjchem-1125	196	88	(	(	PUNCT
eurjchem-1125	196	89	38.7	38.7	NUM
eurjchem-1125	196	90	)	)	PUNCT
eurjchem-1125	196	91	,	,	PUNCT
eurjchem-1125	196	92	90	90	NUM
eurjchem-1125	196	93	(	(	PUNCT
eurjchem-1125	196	94	45.1	45.1	NUM
eurjchem-1125	196	95	)	)	PUNCT
eurjchem-1125	196	96	,	,	PUNCT
eurjchem-1125	196	97	77	77	NUM
eurjchem-1125	196	98	(	(	PUNCT
eurjchem-1125	196	99	100	100	NUM
eurjchem-1125	196	100	)	)	PUNCT
eurjchem-1125	196	101	,	,	PUNCT
eurjchem-1125	196	102	68	68	NUM
eurjchem-1125	196	103	(	(	PUNCT
eurjchem-1125	196	104	41.7	41.7	NUM
eurjchem-1125	196	105	)	)	PUNCT
eurjchem-1125	196	106	,	,	PUNCT
eurjchem-1125	196	107	57	57	NUM
eurjchem-1125	196	108	(	(	PUNCT
eurjchem-1125	196	109	86.6	86.6	NUM
eurjchem-1125	196	110	)	)	PUNCT
eurjchem-1125	196	111	.	.	PUNCT
eurjchem-1125	197	1	anal	anal	PROPN
eurjchem-1125	197	2	.	.	PUNCT
eurjchem-1125	197	3	calcd	calcd	NOUN
eurjchem-1125	197	4	.	.	PUNCT
eurjchem-1125	198	1	for	for	ADP
eurjchem-1125	198	2	c23h28n2o7s3	c23h28n2o7s3	ADJ
eurjchem-1125	198	3	:	:	PUNCT
eurjchem-1125	198	4	c	c	X
eurjchem-1125	198	5	,	,	PUNCT
eurjchem-1125	198	6	51.09	51.09	NUM
eurjchem-1125	198	7	;	;	PUNCT
eurjchem-1125	198	8	h	h	X
eurjchem-1125	198	9	,	,	PUNCT
eurjchem-1125	198	10	5.22	5.22	NUM
eurjchem-1125	198	11	;	;	PUNCT
eurjchem-1125	198	12	n	n	CCONJ
eurjchem-1125	198	13	,	,	PUNCT
eurjchem-1125	198	14	5.18	5.18	NUM
eurjchem-1125	198	15	.	.	PUNCT
eurjchem-1125	198	16	found	find	VERB
eurjchem-1125	198	17	:	:	PUNCT
eurjchem-1125	198	18	51.05	51.05	NUM
eurjchem-1125	198	19	;	;	PUNCT
eurjchem-1125	198	20	h	h	NOUN
eurjchem-1125	198	21	,	,	PUNCT
eurjchem-1125	198	22	5.26	5.26	NUM
eurjchem-1125	198	23	;	;	PUNCT
eurjchem-1125	198	24	n	n	CCONJ
eurjchem-1125	198	25	,	,	PUNCT
eurjchem-1125	198	26	5.15	5.15	NUM
eurjchem-1125	198	27	%	%	NOUN
eurjchem-1125	198	28	.	.	PUNCT
eurjchem-1125	199	1	2.2.9	2.2.9	X
eurjchem-1125	199	2	.	.	PUNCT
eurjchem-1125	200	1	synthesis	synthesis	NOUN
eurjchem-1125	200	2	of	of	ADP
eurjchem-1125	200	3	ethyl	ethyl	PROPN
eurjchem-1125	200	4	2‐(2‐cyano‐2‐(4‐methyl‐3‐phenyl	2‐(2‐cyano‐2‐(4‐methyl‐3‐phenyl	X
eurjchem-1125	201	1	thiazol‐2(3h)‐ylidene)acetamido)‐4,5,6,7‐tetrahydrobenzo‐	thiazol‐2(3h)‐ylidene)acetamido)‐4,5,6,7‐tetrahydrobenzo‐	X
eurjchem-1125	202	1	[	[	X
eurjchem-1125	202	2	b]thiophene‐3‐carboxylate	b]thiophene‐3‐carboxylate	X
eurjchem-1125	202	3	(	(	PUNCT
eurjchem-1125	202	4	19	19	NUM
eurjchem-1125	202	5	)	)	PUNCT
eurjchem-1125	202	6	and	and	CCONJ
eurjchem-1125	202	7	ethyl	ethyl	PROPN
eurjchem-1125	202	8	2‐(2‐cyano‐2‐(4‐	2‐(2‐cyano‐2‐(4‐	NUM
eurjchem-1125	202	9	oxo‐3‐phenylthiazolidin‐2‐ylidene)acetamido)‐4,5,6,7‐tetra	oxo‐3‐phenylthiazolidin‐2‐ylidene)acetamido)‐4,5,6,7‐tetra	PROPN
eurjchem-1125	202	10	hydrobenzo[b]thiophene‐3‐carboxylate	hydrobenzo[b]thiophene‐3‐carboxylate	NOUN
eurjchem-1125	202	11	(	(	PUNCT
eurjchem-1125	202	12	20	20	NUM
eurjchem-1125	202	13	)	)	PUNCT
eurjchem-1125	202	14	to	to	ADP
eurjchem-1125	202	15	a	a	DET
eurjchem-1125	202	16	cold	cold	ADJ
eurjchem-1125	202	17	suspension	suspension	NOUN
eurjchem-1125	202	18	of	of	ADP
eurjchem-1125	202	19	finely	finely	ADV
eurjchem-1125	202	20	divided	divide	VERB
eurjchem-1125	202	21	koh	koh	PROPN
eurjchem-1125	202	22	(	(	PUNCT
eurjchem-1125	202	23	0.11	0.11	NUM
eurjchem-1125	202	24	g	g	NOUN
eurjchem-1125	202	25	,	,	PUNCT
eurjchem-1125	202	26	2	2	NUM
eurjchem-1125	202	27	mmol	mmol	NOUN
eurjchem-1125	202	28	)	)	PUNCT
eurjchem-1125	202	29	in	in	ADP
eurjchem-1125	202	30	dry	dry	ADJ
eurjchem-1125	202	31	dimethylformamide	dimethylformamide	NOUN
eurjchem-1125	202	32	(	(	PUNCT
eurjchem-1125	202	33	10	10	NUM
eurjchem-1125	202	34	ml	ml	NOUN
eurjchem-1125	202	35	)	)	PUNCT
eurjchem-1125	202	36	,	,	PUNCT
eurjchem-1125	202	37	the	the	DET
eurjchem-1125	202	38	cyanoacetamide	cyanoacetamide	ADJ
eurjchem-1125	202	39	derivative	derivative	ADJ
eurjchem-1125	202	40	3	3	NUM
eurjchem-1125	202	41	(	(	PUNCT
eurjchem-1125	202	42	0.58	0.58	NUM
eurjchem-1125	202	43	g	g	NOUN
eurjchem-1125	202	44	,	,	PUNCT
eurjchem-1125	202	45	2	2	NUM
eurjchem-1125	202	46	mmol	mmol	NOUN
eurjchem-1125	202	47	)	)	PUNCT
eurjchem-1125	202	48	followed	follow	VERB
eurjchem-1125	202	49	by	by	ADP
eurjchem-1125	202	50	phenyl	phenyl	NOUN
eurjchem-1125	202	51	isothio	isothio	PROPN
eurjchem-1125	202	52	cyanate	cyanate	NOUN
eurjchem-1125	202	53	(	(	PUNCT
eurjchem-1125	202	54	0.27	0.27	NUM
eurjchem-1125	202	55	g	g	NOUN
eurjchem-1125	202	56	,	,	PUNCT
eurjchem-1125	202	57	2	2	NUM
eurjchem-1125	202	58	mmol	mmol	NOUN
eurjchem-1125	202	59	)	)	PUNCT
eurjchem-1125	202	60	was	be	AUX
eurjchem-1125	202	61	added	add	VERB
eurjchem-1125	202	62	.	.	PUNCT
eurjchem-1125	203	1	the	the	DET
eurjchem-1125	203	2	mixture	mixture	NOUN
eurjchem-1125	203	3	was	be	AUX
eurjchem-1125	203	4	stirred	stir	VERB
eurjchem-1125	203	5	at	at	ADP
eurjchem-1125	203	6	room	room	NOUN
eurjchem-1125	203	7	temperature	temperature	NOUN
eurjchem-1125	203	8	for	for	ADP
eurjchem-1125	203	9	12	12	NUM
eurjchem-1125	203	10	h	h	NOUN
eurjchem-1125	203	11	,	,	PUNCT
eurjchem-1125	203	12	and	and	CCONJ
eurjchem-1125	203	13	then	then	ADV
eurjchem-1125	203	14	cooled	cool	VERB
eurjchem-1125	203	15	again	again	ADV
eurjchem-1125	203	16	to	to	ADP
eurjchem-1125	203	17	5‐0	5‐0	NUM
eurjchem-1125	203	18	°	°	ADP
eurjchem-1125	203	19	c	c	NOUN
eurjchem-1125	203	20	,	,	PUNCT
eurjchem-1125	203	21	treated	treat	VERB
eurjchem-1125	203	22	with	with	ADP
eurjchem-1125	203	23	the	the	DET
eurjchem-1125	203	24	chloroacetone	chloroacetone	NOUN
eurjchem-1125	203	25	(	(	PUNCT
eurjchem-1125	203	26	0.18	0.18	NUM
eurjchem-1125	203	27	g	g	NOUN
eurjchem-1125	203	28	,	,	PUNCT
eurjchem-1125	203	29	2	2	NUM
eurjchem-1125	203	30	mmol	mmol	NOUN
eurjchem-1125	203	31	)	)	PUNCT
eurjchem-1125	203	32	or	or	CCONJ
eurjchem-1125	203	33	ethyl	ethyl	PROPN
eurjchem-1125	203	34	bromoacetate	bromoacetate	NOUN
eurjchem-1125	203	35	(	(	PUNCT
eurjchem-1125	203	36	0.24	0.24	NUM
eurjchem-1125	203	37	g	g	NOUN
eurjchem-1125	203	38	,	,	PUNCT
eurjchem-1125	203	39	2	2	NUM
eurjchem-1125	203	40	mmol	mmol	NOUN
eurjchem-1125	203	41	)	)	PUNCT
eurjchem-1125	203	42	and	and	CCONJ
eurjchem-1125	203	43	left	leave	VERB
eurjchem-1125	203	44	to	to	PART
eurjchem-1125	203	45	stand	stand	VERB
eurjchem-1125	203	46	at	at	ADP
eurjchem-1125	203	47	room	room	NOUN
eurjchem-1125	203	48	temperature	temperature	NOUN
eurjchem-1125	203	49	for	for	ADP
eurjchem-1125	203	50	24	24	NUM
eurjchem-1125	203	51	h	h	NOUN
eurjchem-1125	203	52	,	,	PUNCT
eurjchem-1125	203	53	the	the	DET
eurjchem-1125	203	54	mixture	mixture	NOUN
eurjchem-1125	203	55	was	be	AUX
eurjchem-1125	203	56	poured	pour	VERB
eurjchem-1125	203	57	into	into	ADP
eurjchem-1125	203	58	ice	ice	NOUN
eurjchem-1125	203	59	cold	cold	ADJ
eurjchem-1125	203	60	water	water	NOUN
eurjchem-1125	203	61	.	.	PUNCT
eurjchem-1125	204	1	the	the	DET
eurjchem-1125	204	2	resulting	result	VERB
eurjchem-1125	204	3	precipitate	precipitate	NOUN
eurjchem-1125	204	4	was	be	AUX
eurjchem-1125	204	5	filtered	filter	VERB
eurjchem-1125	204	6	off	off	ADP
eurjchem-1125	204	7	,	,	PUNCT
eurjchem-1125	204	8	dried	dry	VERB
eurjchem-1125	204	9	and	and	CCONJ
eurjchem-1125	204	10	crystallized	crystallize	VERB
eurjchem-1125	204	11	from	from	ADP
eurjchem-1125	204	12	dmf	dmf	PROPN
eurjchem-1125	204	13	:	:	PUNCT
eurjchem-1125	204	14	ethanol	ethanol	NOUN
eurjchem-1125	204	15	(	(	PUNCT
eurjchem-1125	204	16	5:2	5:2	NUM
eurjchem-1125	204	17	,	,	PUNCT
eurjchem-1125	204	18	v	v	NOUN
eurjchem-1125	204	19	:	:	PUNCT
eurjchem-1125	204	20	v	v	NOUN
eurjchem-1125	204	21	)	)	PUNCT
eurjchem-1125	204	22	mixture	mixture	NOUN
eurjchem-1125	204	23	to	to	PART
eurjchem-1125	204	24	afford	afford	VERB
eurjchem-1125	204	25	compounds	compound	NOUN
eurjchem-1125	204	26	19	19	NUM
eurjchem-1125	204	27	and	and	CCONJ
eurjchem-1125	204	28	20	20	NUM
eurjchem-1125	204	29	,	,	PUNCT
eurjchem-1125	204	30	respectively	respectively	ADV
eurjchem-1125	204	31	(	(	PUNCT
eurjchem-1125	204	32	scheme	scheme	NOUN
eurjchem-1125	204	33	5	5	NUM
eurjchem-1125	204	34	)	)	PUNCT
eurjchem-1125	204	35	.	.	PUNCT
eurjchem-1125	205	1	ethyl	ethyl	PROPN
eurjchem-1125	205	2	2‐{[(2z)‐2‐cyano‐2‐(4‐methyl‐3‐phenyl‐1	2‐{[(2z)‐2‐cyano‐2‐(4‐methyl‐3‐phenyl‐1	NUM
eurjchem-1125	205	3	,	,	PUNCT
eurjchem-1125	205	4	3‐thiazol‐	3‐thiazol‐	NUM
eurjchem-1125	205	5	2(3h)‐ylidene)acetyl]amino}‐4	2(3h)‐ylidene)acetyl]amino}‐4	NOUN
eurjchem-1125	205	6	,	,	PUNCT
eurjchem-1125	205	7	5	5	NUM
eurjchem-1125	205	8	,	,	PUNCT
eurjchem-1125	205	9	6	6	NUM
eurjchem-1125	205	10	,	,	PUNCT
eurjchem-1125	205	11	7‐tetrahydro‐1‐benzothio	7‐tetrahydro‐1‐benzothio	NUM
eurjchem-1125	205	12	phene‐3‐carboxylate	phene‐3‐carboxylate	NOUN
eurjchem-1125	205	13	(	(	PUNCT
eurjchem-1125	205	14	19	19	NUM
eurjchem-1125	205	15	):	):	PUNCT
eurjchem-1125	205	16	color	color	NOUN
eurjchem-1125	205	17	:	:	PUNCT
eurjchem-1125	205	18	pale	pale	ADJ
eurjchem-1125	205	19	yellow	yellow	ADJ
eurjchem-1125	205	20	powder	powder	NOUN
eurjchem-1125	205	21	.	.	PUNCT
eurjchem-1125	206	1	yield	yield	VERB
eurjchem-1125	206	2	0.59	0.59	NUM
eurjchem-1125	206	3	g	g	NOUN
eurjchem-1125	206	4	,	,	PUNCT
eurjchem-1125	206	5	63	63	NUM
eurjchem-1125	206	6	%	%	NOUN
eurjchem-1125	206	7	.	.	PUNCT
eurjchem-1125	207	1	m.p	m.p	PROPN
eurjchem-1125	207	2	.	.	PROPN
eurjchem-1125	207	3	:	:	PUNCT
eurjchem-1125	208	1	206	206	NUM
eurjchem-1125	208	2	°	°	SYM
eurjchem-1125	208	3	c	c	X
eurjchem-1125	208	4	.	.	PUNCT
eurjchem-1125	209	1	(	(	PUNCT
eurjchem-1125	209	2	lit	light	VERB
eurjchem-1125	209	3	.	.	PUNCT
eurjchem-1125	210	1	[	[	X
eurjchem-1125	210	2	8	8	NUM
eurjchem-1125	210	3	]	]	PUNCT
eurjchem-1125	210	4	,	,	PUNCT
eurjchem-1125	210	5	205	205	NUM
eurjchem-1125	210	6	°	°	NOUN
eurjchem-1125	210	7	c	c	NOUN
eurjchem-1125	210	8	)	)	PUNCT
eurjchem-1125	210	9	.	.	PUNCT
eurjchem-1125	210	10	ethyl	ethyl	PROPN
eurjchem-1125	210	11	2‐(2‐cyano‐2‐(4‐oxo‐3‐phenylthiazolidin‐2‐ylidene)acet	2‐(2‐cyano‐2‐(4‐oxo‐3‐phenylthiazolidin‐2‐ylidene)acet	NUM
eurjchem-1125	211	1	amido)‐4	amido)‐4	ADJ
eurjchem-1125	211	2	,	,	PUNCT
eurjchem-1125	211	3	5	5	NUM
eurjchem-1125	211	4	,	,	PUNCT
eurjchem-1125	211	5	6	6	NUM
eurjchem-1125	211	6	,	,	PUNCT
eurjchem-1125	211	7	7‐tetrahydrobenzo[b]thiophene‐3‐carboxylate	7‐tetrahydrobenzo[b]thiophene‐3‐carboxylate	NUM
eurjchem-1125	211	8	(	(	PUNCT
eurjchem-1125	211	9	20	20	NUM
eurjchem-1125	211	10	):	):	PUNCT
eurjchem-1125	211	11	color	color	NOUN
eurjchem-1125	211	12	:	:	PUNCT
eurjchem-1125	211	13	brown	brown	ADJ
eurjchem-1125	211	14	powder	powder	NOUN
eurjchem-1125	211	15	.	.	PUNCT
eurjchem-1125	212	1	yield	yield	NOUN
eurjchem-1125	212	2	:	:	PUNCT
eurjchem-1125	212	3	0.51	0.51	NUM
eurjchem-1125	212	4	g	g	NOUN
eurjchem-1125	212	5	,	,	PUNCT
eurjchem-1125	212	6	55	55	NUM
eurjchem-1125	212	7	%	%	NOUN
eurjchem-1125	212	8	.	.	PUNCT
eurjchem-1125	213	1	m.p	m.p	PROPN
eurjchem-1125	213	2	.	.	PROPN
eurjchem-1125	213	3	:	:	PUNCT
eurjchem-1125	214	1	>	>	X
eurjchem-1125	214	2	320	320	NUM
eurjchem-1125	214	3	°	°	NOUN
eurjchem-1125	214	4	c	c	NOUN
eurjchem-1125	214	5	.	.	PUNCT
eurjchem-1125	215	1	(	(	PUNCT
eurjchem-1125	215	2	lit	light	VERB
eurjchem-1125	215	3	.	.	PUNCT
eurjchem-1125	216	1	[	[	X
eurjchem-1125	216	2	8	8	X
eurjchem-1125	216	3	]	]	PUNCT
eurjchem-1125	216	4	>	>	X
eurjchem-1125	216	5	320	320	NUM
eurjchem-1125	216	6	°	°	NOUN
eurjchem-1125	216	7	c	c	NOUN
eurjchem-1125	216	8	)	)	PUNCT
eurjchem-1125	216	9	.	.	PUNCT
eurjchem-1125	217	1	2.2.10	2.2.10	NUM
eurjchem-1125	217	2	.	.	PUNCT
eurjchem-1125	218	1	reaction	reaction	NOUN
eurjchem-1125	218	2	of	of	ADP
eurjchem-1125	218	3	ethyl	ethyl	PROPN
eurjchem-1125	218	4	2‐{[(2e)‐3‐anilino‐2‐cyano‐3‐	2‐{[(2e)‐3‐anilino‐2‐cyano‐3‐	NUM
eurjchem-1125	218	5	mercaptoprop‐2‐enoyl]amino}‐4,5,6,7‐tetrahydro‐1‐benzo	mercaptoprop‐2‐enoyl]amino}‐4,5,6,7‐tetrahydro‐1‐benzo	NOUN
eurjchem-1125	218	6	thiophene‐3‐carboxylate	thiophene‐3‐carboxylate	NUM
eurjchem-1125	218	7	(	(	PUNCT
eurjchem-1125	218	8	23	23	NUM
eurjchem-1125	218	9	)	)	PUNCT
eurjchem-1125	218	10	with	with	ADP
eurjchem-1125	218	11	α‐halogen	α‐halogen	PART
eurjchem-1125	218	12	carbonyl	carbonyl	NOUN
eurjchem-1125	218	13	compounds	compound	NOUN
eurjchem-1125	218	14	chloroacetone	chloroacetone	NOUN
eurjchem-1125	218	15	(	(	PUNCT
eurjchem-1125	218	16	0.18	0.18	NUM
eurjchem-1125	218	17	g	g	NOUN
eurjchem-1125	218	18	,	,	PUNCT
eurjchem-1125	218	19	2	2	NUM
eurjchem-1125	218	20	mmol	mmol	NOUN
eurjchem-1125	218	21	)	)	PUNCT
eurjchem-1125	218	22	or	or	CCONJ
eurjchem-1125	218	23	ethyl	ethyl	PROPN
eurjchem-1125	218	24	bromoacetate	bromoacetate	NOUN
eurjchem-1125	218	25	was	be	AUX
eurjchem-1125	218	26	added	add	VERB
eurjchem-1125	218	27	in	in	ADP
eurjchem-1125	218	28	solution	solution	NOUN
eurjchem-1125	218	29	containing	contain	VERB
eurjchem-1125	218	30	ethanol	ethanol	NOUN
eurjchem-1125	218	31	(	(	PUNCT
eurjchem-1125	218	32	10	10	NUM
eurjchem-1125	218	33	ml	ml	NOUN
eurjchem-1125	218	34	)	)	PUNCT
eurjchem-1125	218	35	,	,	PUNCT
eurjchem-1125	218	36	triethylamine	triethylamine	NOUN
eurjchem-1125	218	37	(	(	PUNCT
eurjchem-1125	218	38	0.2	0.2	NUM
eurjchem-1125	218	39	ml	ml	NOUN
eurjchem-1125	218	40	)	)	PUNCT
eurjchem-1125	218	41	and	and	CCONJ
eurjchem-1125	218	42	compound	compound	VERB
eurjchem-1125	218	43	23	23	NUM
eurjchem-1125	218	44	(	(	PUNCT
eurjchem-1125	218	45	0.86	0.86	NUM
eurjchem-1125	218	46	g	g	NOUN
eurjchem-1125	218	47	,	,	PUNCT
eurjchem-1125	218	48	2	2	NUM
eurjchem-1125	218	49	mmole	mmole	NOUN
eurjchem-1125	218	50	)	)	PUNCT
eurjchem-1125	218	51	.	.	PUNCT
eurjchem-1125	219	1	the	the	DET
eurjchem-1125	219	2	reaction	reaction	NOUN
eurjchem-1125	219	3	mixture	mixture	NOUN
eurjchem-1125	219	4	was	be	AUX
eurjchem-1125	219	5	refluxed	refluxe	VERB
eurjchem-1125	219	6	for	for	ADP
eurjchem-1125	219	7	3	3	NUM
eurjchem-1125	219	8	h.	h.	NOUN
eurjchem-1125	219	9	the	the	DET
eurjchem-1125	219	10	obtained	obtain	VERB
eurjchem-1125	219	11	product	product	NOUN
eurjchem-1125	219	12	after	after	SCONJ
eurjchem-1125	219	13	addition	addition	NOUN
eurjchem-1125	219	14	of	of	ADP
eurjchem-1125	219	15	water	water	NOUN
eurjchem-1125	219	16	was	be	AUX
eurjchem-1125	219	17	filtered	filter	VERB
eurjchem-1125	219	18	,	,	PUNCT
eurjchem-1125	219	19	dried	dry	VERB
eurjchem-1125	219	20	and	and	CCONJ
eurjchem-1125	219	21	crystallized	crystallize	VERB
eurjchem-1125	219	22	from	from	ADP
eurjchem-1125	219	23	ethanol	ethanol	NOUN
eurjchem-1125	219	24	:	:	PUNCT
eurjchem-1125	219	25	benzene	benzene	NOUN
eurjchem-1125	219	26	(	(	PUNCT
eurjchem-1125	219	27	1	1	NUM
eurjchem-1125	219	28	:	:	SYM
eurjchem-1125	219	29	3	3	NUM
eurjchem-1125	219	30	,	,	PUNCT
eurjchem-1125	219	31	v	v	NOUN
eurjchem-1125	219	32	:	:	SYM
eurjchem-1125	219	33	v	v	NOUN
eurjchem-1125	219	34	)	)	PUNCT
eurjchem-1125	219	35	to	to	PART
eurjchem-1125	219	36	give	give	VERB
eurjchem-1125	219	37	compounds	compound	NOUN
eurjchem-1125	219	38	24	24	NUM
eurjchem-1125	219	39	and	and	CCONJ
eurjchem-1125	219	40	25	25	NUM
eurjchem-1125	219	41	,	,	PUNCT
eurjchem-1125	219	42	respectively	respectively	ADV
eurjchem-1125	219	43	(	(	PUNCT
eurjchem-1125	219	44	scheme	scheme	NOUN
eurjchem-1125	219	45	5	5	NUM
eurjchem-1125	219	46	)	)	PUNCT
eurjchem-1125	219	47	.	.	PUNCT
eurjchem-1125	220	1	ethyl	ethyl	PROPN
eurjchem-1125	220	2	2‐{[(5‐acetyl‐4‐amino‐2‐anilino‐3‐thienyl	2‐{[(5‐acetyl‐4‐amino‐2‐anilino‐3‐thienyl	NUM
eurjchem-1125	220	3	)	)	PUNCT
eurjchem-1125	220	4	carbonyl	carbonyl	NOUN
eurjchem-1125	220	5	]	]	PUNCT
eurjchem-1125	220	6	amino}‐4	amino}‐4	NOUN
eurjchem-1125	220	7	,	,	PUNCT
eurjchem-1125	220	8	5	5	NUM
eurjchem-1125	220	9	,	,	PUNCT
eurjchem-1125	220	10	6	6	NUM
eurjchem-1125	220	11	,	,	PUNCT
eurjchem-1125	220	12	7‐tetrahydro‐1‐benzothiophene‐3‐carboxylate	7‐tetrahydro‐1‐benzothiophene‐3‐carboxylate	PROPN
eurjchem-1125	220	13	(	(	PUNCT
eurjchem-1125	220	14	24	24	NUM
eurjchem-1125	220	15	):	):	PUNCT
eurjchem-1125	220	16	color	color	NOUN
eurjchem-1125	220	17	:	:	PUNCT
eurjchem-1125	220	18	brown	brown	ADJ
eurjchem-1125	220	19	crystals	crystal	NOUN
eurjchem-1125	220	20	.	.	PUNCT
eurjchem-1125	221	1	yield	yield	VERB
eurjchem-1125	221	2	0.67	0.67	NUM
eurjchem-1125	221	3	g	g	NOUN
eurjchem-1125	221	4	,	,	PUNCT
eurjchem-1125	221	5	69	69	NUM
eurjchem-1125	221	6	%	%	NOUN
eurjchem-1125	221	7	.	.	PUNCT
eurjchem-1125	222	1	m.p	m.p	PROPN
eurjchem-1125	222	2	.	.	PROPN
eurjchem-1125	222	3	:	:	PUNCT
eurjchem-1125	223	1	230	230	NUM
eurjchem-1125	223	2	°	°	NUM
eurjchem-1125	223	3	c	c	X
eurjchem-1125	223	4	.	.	PUNCT
eurjchem-1125	224	1	ft‐	ft‐	PROPN
eurjchem-1125	224	2	ir	ir	NOUN
eurjchem-1125	224	3	:	:	PUNCT
eurjchem-1125	224	4	3234	3234	NUM
eurjchem-1125	224	5	(	(	PUNCT
eurjchem-1125	224	6	nh	nh	PROPN
eurjchem-1125	224	7	,	,	PUNCT
eurjchem-1125	224	8	nh2	nh2	PROPN
eurjchem-1125	224	9	,	,	PUNCT
eurjchem-1125	224	10	br	br	PROPN
eurjchem-1125	224	11	)	)	PUNCT
eurjchem-1125	224	12	,	,	PUNCT
eurjchem-1125	224	13	1671	1671	NUM
eurjchem-1125	224	14	,	,	PUNCT
eurjchem-1125	224	15	1610	1610	NUM
eurjchem-1125	224	16	(	(	PUNCT
eurjchem-1125	224	17	c	c	NOUN
eurjchem-1125	224	18	=	=	NOUN
eurjchem-1125	224	19	o	o	NOUN
eurjchem-1125	224	20	)	)	PUNCT
eurjchem-1125	224	21	.	.	PUNCT
eurjchem-1125	225	1	1h	1h	NUM
eurjchem-1125	225	2	nmr	nmr	NOUN
eurjchem-1125	225	3	(	(	PUNCT
eurjchem-1125	225	4	400	400	NUM
eurjchem-1125	225	5	mhz	mhz	NOUN
eurjchem-1125	225	6	,	,	PUNCT
eurjchem-1125	225	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1125	225	8	,	,	PUNCT
eurjchem-1125	225	9	δ	δ	PROPN
eurjchem-1125	225	10	,	,	PUNCT
eurjchem-1125	225	11	ppm	ppm	NUM
eurjchem-1125	225	12	):	):	PUNCT
eurjchem-1125	225	13	1.21	1.21	NUM
eurjchem-1125	225	14	(	(	PUNCT
eurjchem-1125	225	15	t	t	PROPN
eurjchem-1125	225	16	,	,	PUNCT
eurjchem-1125	225	17	3h	3h	NUM
eurjchem-1125	225	18	,	,	PUNCT
eurjchem-1125	225	19	j	j	PROPN
eurjchem-1125	225	20	=	=	SYM
eurjchem-1125	225	21	7.2	7.2	NUM
eurjchem-1125	225	22	hz	hz	NOUN
eurjchem-1125	225	23	,	,	PUNCT
eurjchem-1125	225	24	ch3	ch3	PROPN
eurjchem-1125	225	25	)	)	PUNCT
eurjchem-1125	225	26	,	,	PUNCT
eurjchem-1125	225	27	1.74‐1.90	1.74‐1.90	NUM
eurjchem-1125	225	28	(	(	PUNCT
eurjchem-1125	225	29	m	m	PROPN
eurjchem-1125	225	30	,	,	PUNCT
eurjchem-1125	225	31	4h	4h	NOUN
eurjchem-1125	225	32	,	,	PUNCT
eurjchem-1125	225	33	c5‐2h	c5‐2h	PROPN
eurjchem-1125	225	34	,	,	PUNCT
eurjchem-1125	225	35	c6‐2h	c6‐2h	NOUN
eurjchem-1125	225	36	)	)	PUNCT
eurjchem-1125	225	37	,	,	PUNCT
eurjchem-1125	225	38	2.10	2.10	NUM
eurjchem-1125	225	39	(	(	PUNCT
eurjchem-1125	225	40	s	s	PROPN
eurjchem-1125	225	41	,	,	PUNCT
eurjchem-1125	225	42	3h	3h	NUM
eurjchem-1125	225	43	,	,	PUNCT
eurjchem-1125	225	44	ch3	ch3	PROPN
eurjchem-1125	225	45	)	)	PUNCT
eurjchem-1125	225	46	,	,	PUNCT
eurjchem-1125	225	47	2.63‐2.77	2.63‐2.77	NUM
eurjchem-1125	225	48	(	(	PUNCT
eurjchem-1125	225	49	m	m	PROPN
eurjchem-1125	225	50	,	,	PUNCT
eurjchem-1125	225	51	4h	4h	NUM
eurjchem-1125	225	52	,	,	PUNCT
eurjchem-1125	225	53	c4‐2h	c4‐2h	PROPN
eurjchem-1125	225	54	,	,	PUNCT
eurjchem-1125	225	55	c7‐	c7‐	ADJ
eurjchem-1125	225	56	2h	2h	NUM
eurjchem-1125	225	57	)	)	PUNCT
eurjchem-1125	225	58	,	,	PUNCT
eurjchem-1125	225	59	4.42	4.42	NUM
eurjchem-1125	225	60	(	(	PUNCT
eurjchem-1125	225	61	q	q	NOUN
eurjchem-1125	225	62	,	,	PUNCT
eurjchem-1125	225	63	2h	2h	NUM
eurjchem-1125	225	64	,	,	PUNCT
eurjchem-1125	225	65	j	j	PROPN
eurjchem-1125	226	1	=	=	SYM
eurjchem-1125	226	2	7.2	7.2	NUM
eurjchem-1125	226	3	hz	hz	NOUN
eurjchem-1125	226	4	,	,	PUNCT
eurjchem-1125	226	5	ch2o	ch2o	NOUN
eurjchem-1125	226	6	)	)	PUNCT
eurjchem-1125	226	7	,	,	PUNCT
eurjchem-1125	226	8	7.1‐7.5	7.1‐7.5	NUM
eurjchem-1125	226	9	(	(	PUNCT
eurjchem-1125	226	10	m	m	PROPN
eurjchem-1125	226	11	,	,	PUNCT
eurjchem-1125	226	12	8h	8h	PROPN
eurjchem-1125	226	13	,	,	PUNCT
eurjchem-1125	226	14	nh2	nh2	PROPN
eurjchem-1125	226	15	,	,	PUNCT
eurjchem-1125	226	16	nh	nh	PROPN
eurjchem-1125	226	17	,	,	PUNCT
eurjchem-1125	226	18	ar‐	ar‐	PROPN
eurjchem-1125	226	19	h	h	NOUN
eurjchem-1125	226	20	)	)	PUNCT
eurjchem-1125	226	21	,	,	PUNCT
eurjchem-1125	226	22	11.82	11.82	NUM
eurjchem-1125	226	23	(	(	PUNCT
eurjchem-1125	226	24	s	s	PROPN
eurjchem-1125	226	25	,	,	PUNCT
eurjchem-1125	226	26	1h	1h	NUM
eurjchem-1125	226	27	,	,	PUNCT
eurjchem-1125	226	28	nh‐co	nh‐co	NUM
eurjchem-1125	226	29	)	)	PUNCT
eurjchem-1125	226	30	.	.	PUNCT
eurjchem-1125	227	1	ei‐ms	ei‐ms	PROPN
eurjchem-1125	227	2	(	(	PUNCT
eurjchem-1125	227	3	m	m	NOUN
eurjchem-1125	227	4	/	/	SYM
eurjchem-1125	227	5	z	z	NOUN
eurjchem-1125	227	6	(	(	PUNCT
eurjchem-1125	227	7	%	%	NOUN
eurjchem-1125	227	8	)	)	PUNCT
eurjchem-1125	227	9	):	):	PUNCT
eurjchem-1125	227	10	484	484	NUM
eurjchem-1125	227	11	(	(	PUNCT
eurjchem-1125	227	12	m++1	m++1	NOUN
eurjchem-1125	227	13	,	,	PUNCT
eurjchem-1125	227	14	8.9	8.9	NUM
eurjchem-1125	227	15	)	)	PUNCT
eurjchem-1125	227	16	,	,	PUNCT
eurjchem-1125	227	17	451	451	NUM
eurjchem-1125	227	18	(	(	PUNCT
eurjchem-1125	227	19	6.9	6.9	NUM
eurjchem-1125	227	20	)	)	PUNCT
eurjchem-1125	227	21	,	,	PUNCT
eurjchem-1125	227	22	437	437	NUM
eurjchem-1125	227	23	(	(	PUNCT
eurjchem-1125	227	24	7.6	7.6	NUM
eurjchem-1125	227	25	)	)	PUNCT
eurjchem-1125	227	26	,	,	PUNCT
eurjchem-1125	227	27	259	259	NUM
eurjchem-1125	227	28	(	(	PUNCT
eurjchem-1125	227	29	15.0	15.0	NUM
eurjchem-1125	227	30	)	)	PUNCT
eurjchem-1125	227	31	,	,	PUNCT
eurjchem-1125	227	32	242	242	NUM
eurjchem-1125	227	33	(	(	PUNCT
eurjchem-1125	227	34	22.0	22.0	NUM
eurjchem-1125	227	35	)	)	PUNCT
eurjchem-1125	227	36	,	,	PUNCT
eurjchem-1125	227	37	225	225	NUM
eurjchem-1125	227	38	(	(	PUNCT
eurjchem-1125	227	39	41.0	41.0	NUM
eurjchem-1125	227	40	)	)	PUNCT
eurjchem-1125	227	41	,	,	PUNCT
eurjchem-1125	227	42	216	216	NUM
eurjchem-1125	227	43	(	(	PUNCT
eurjchem-1125	227	44	47.9	47.9	NUM
eurjchem-1125	227	45	)	)	PUNCT
eurjchem-1125	227	46	,	,	PUNCT
eurjchem-1125	227	47	178	178	NUM
eurjchem-1125	227	48	(	(	PUNCT
eurjchem-1125	227	49	100	100	NUM
eurjchem-1125	227	50	)	)	PUNCT
eurjchem-1125	227	51	,	,	PUNCT
eurjchem-1125	227	52	150	150	NUM
eurjchem-1125	227	53	(	(	PUNCT
eurjchem-1125	227	54	66.1	66.1	NUM
eurjchem-1125	227	55	)	)	PUNCT
eurjchem-1125	227	56	,	,	PUNCT
eurjchem-1125	227	57	143	143	NUM
eurjchem-1125	227	58	(	(	PUNCT
eurjchem-1125	227	59	37.7	37.7	NUM
eurjchem-1125	227	60	)	)	PUNCT
eurjchem-1125	227	61	,	,	PUNCT
eurjchem-1125	227	62	121	121	NUM
eurjchem-1125	227	63	(	(	PUNCT
eurjchem-1125	227	64	41.5	41.5	NUM
eurjchem-1125	227	65	)	)	PUNCT
eurjchem-1125	227	66	,	,	PUNCT
eurjchem-1125	227	67	116	116	NUM
eurjchem-1125	227	68	(	(	PUNCT
eurjchem-1125	227	69	37.0	37.0	NUM
eurjchem-1125	227	70	)	)	PUNCT
eurjchem-1125	227	71	,	,	PUNCT
eurjchem-1125	227	72	90	90	NUM
eurjchem-1125	227	73	(	(	PUNCT
eurjchem-1125	227	74	36.7	36.7	NUM
eurjchem-1125	227	75	)	)	PUNCT
eurjchem-1125	227	76	,	,	PUNCT
eurjchem-1125	227	77	76	76	NUM
eurjchem-1125	227	78	(	(	PUNCT
eurjchem-1125	227	79	64.9	64.9	NUM
eurjchem-1125	227	80	)	)	PUNCT
eurjchem-1125	227	81	,	,	PUNCT
eurjchem-1125	227	82	50	50	NUM
eurjchem-1125	227	83	(	(	PUNCT
eurjchem-1125	227	84	25.8	25.8	NUM
eurjchem-1125	227	85	)	)	PUNCT
eurjchem-1125	227	86	.	.	PUNCT
eurjchem-1125	228	1	anal	anal	PROPN
eurjchem-1125	228	2	.	.	PUNCT
eurjchem-1125	228	3	calcd	calcd	NOUN
eurjchem-1125	228	4	.	.	PUNCT
eurjchem-1125	229	1	for	for	ADP
eurjchem-1125	229	2	c24h25n3o4s2	c24h25n3o4s2	NOUN
eurjchem-1125	229	3	:	:	PUNCT
eurjchem-1125	229	4	c	c	X
eurjchem-1125	229	5	,	,	PUNCT
eurjchem-1125	229	6	59.61	59.61	NUM
eurjchem-1125	229	7	;	;	PUNCT
eurjchem-1125	229	8	h	h	NOUN
eurjchem-1125	229	9	,	,	PUNCT
eurjchem-1125	229	10	5.21	5.21	NUM
eurjchem-1125	229	11	;	;	PUNCT
eurjchem-1125	229	12	n	n	CCONJ
eurjchem-1125	229	13	,	,	PUNCT
eurjchem-1125	229	14	8.69	8.69	NUM
eurjchem-1125	229	15	.	.	PUNCT
eurjchem-1125	229	16	found	find	VERB
eurjchem-1125	229	17	:	:	PUNCT
eurjchem-1125	230	1	c	c	X
eurjchem-1125	230	2	,	,	PUNCT
eurjchem-1125	230	3	59.56	59.56	NUM
eurjchem-1125	230	4	;	;	PUNCT
eurjchem-1125	230	5	h	h	NOUN
eurjchem-1125	230	6	,	,	PUNCT
eurjchem-1125	230	7	5.15	5.15	NUM
eurjchem-1125	230	8	;	;	PUNCT
eurjchem-1125	230	9	n	n	CCONJ
eurjchem-1125	230	10	,	,	PUNCT
eurjchem-1125	230	11	8.75	8.75	NUM
eurjchem-1125	230	12	%	%	NOUN
eurjchem-1125	230	13	.	.	PUNCT
eurjchem-1125	231	1	ethyl	ethyl	PROPN
eurjchem-1125	231	2	2‐(3‐amino‐2‐(ethoxycarbonyl)‐5‐(phenylamino)thio	2‐(3‐amino‐2‐(ethoxycarbonyl)‐5‐(phenylamino)thio	PROPN
eurjchem-1125	231	3	phene‐4‐carboxamido)‐4	phene‐4‐carboxamido)‐4	NOUN
eurjchem-1125	231	4	,	,	PUNCT
eurjchem-1125	231	5	5	5	NUM
eurjchem-1125	231	6	,	,	PUNCT
eurjchem-1125	231	7	6	6	NUM
eurjchem-1125	231	8	,	,	PUNCT
eurjchem-1125	231	9	7‐tetrahydrobenzo[b]thiophene‐3‐	7‐tetrahydrobenzo[b]thiophene‐3‐	NUM
eurjchem-1125	231	10	carboxylate	carboxylate	NOUN
eurjchem-1125	231	11	(	(	PUNCT
eurjchem-1125	231	12	25	25	NUM
eurjchem-1125	231	13	):	):	PUNCT
eurjchem-1125	231	14	color	color	NOUN
eurjchem-1125	231	15	:	:	PUNCT
eurjchem-1125	231	16	brown	brown	ADJ
eurjchem-1125	231	17	crystals	crystal	NOUN
eurjchem-1125	231	18	.	.	PUNCT
eurjchem-1125	232	1	yield	yield	VERB
eurjchem-1125	232	2	0.81	0.81	NUM
eurjchem-1125	232	3	g	g	NOUN
eurjchem-1125	232	4	,	,	PUNCT
eurjchem-1125	232	5	79	79	NUM
eurjchem-1125	232	6	%	%	NOUN
eurjchem-1125	232	7	.	.	PUNCT
eurjchem-1125	233	1	m.p	m.p	PROPN
eurjchem-1125	233	2	.	.	PROPN
eurjchem-1125	233	3	:	:	PUNCT
eurjchem-1125	234	1	283	283	NUM
eurjchem-1125	234	2	oc	oc	NOUN
eurjchem-1125	234	3	.	.	PUNCT
eurjchem-1125	234	4	ft‐	ft‐	PROPN
eurjchem-1125	234	5	:	:	PUNCT
eurjchem-1125	234	6	3366	3366	NUM
eurjchem-1125	234	7	,	,	PUNCT
eurjchem-1125	234	8	3200	3200	NUM
eurjchem-1125	234	9	(	(	PUNCT
eurjchem-1125	234	10	nh	nh	PROPN
eurjchem-1125	234	11	,	,	PUNCT
eurjchem-1125	234	12	nh2	nh2	PROPN
eurjchem-1125	234	13	)	)	PUNCT
eurjchem-1125	234	14	,	,	PUNCT
eurjchem-1125	234	15	1664	1664	NUM
eurjchem-1125	234	16	,	,	PUNCT
eurjchem-1125	234	17	1621	1621	NUM
eurjchem-1125	234	18	(	(	PUNCT
eurjchem-1125	234	19	c	c	NOUN
eurjchem-1125	234	20	=	=	NOUN
eurjchem-1125	234	21	o	o	NOUN
eurjchem-1125	234	22	)	)	PUNCT
eurjchem-1125	234	23	.	.	PUNCT
eurjchem-1125	234	24	ei‐ms	ei‐ms	PROPN
eurjchem-1125	234	25	(	(	PUNCT
eurjchem-1125	234	26	m	m	NOUN
eurjchem-1125	234	27	/	/	SYM
eurjchem-1125	234	28	z	z	NOUN
eurjchem-1125	234	29	(	(	PUNCT
eurjchem-1125	234	30	%	%	NOUN
eurjchem-1125	234	31	)	)	PUNCT
eurjchem-1125	234	32	):	):	PUNCT
eurjchem-1125	234	33	515	515	NUM
eurjchem-1125	234	34	(	(	PUNCT
eurjchem-1125	234	35	m++2	m++2	PROPN
eurjchem-1125	234	36	,	,	PUNCT
eurjchem-1125	234	37	1.9	1.9	NUM
eurjchem-1125	234	38	)	)	PUNCT
eurjchem-1125	234	39	,	,	PUNCT
eurjchem-1125	234	40	514	514	NUM
eurjchem-1125	234	41	(	(	PUNCT
eurjchem-1125	234	42	m++1	m++1	NOUN
eurjchem-1125	234	43	,	,	PUNCT
eurjchem-1125	234	44	21.8	21.8	NUM
eurjchem-1125	234	45	)	)	PUNCT
eurjchem-1125	234	46	,	,	PUNCT
eurjchem-1125	234	47	468	468	NUM
eurjchem-1125	234	48	(	(	PUNCT
eurjchem-1125	234	49	18.7	18.7	NUM
eurjchem-1125	234	50	)	)	PUNCT
eurjchem-1125	234	51	,	,	PUNCT
eurjchem-1125	234	52	422	422	NUM
eurjchem-1125	234	53	(	(	PUNCT
eurjchem-1125	234	54	3.5	3.5	NUM
eurjchem-1125	234	55	)	)	PUNCT
eurjchem-1125	234	56	,	,	PUNCT
eurjchem-1125	234	57	394	394	NUM
eurjchem-1125	234	58	(	(	PUNCT
eurjchem-1125	234	59	2.8	2.8	NUM
eurjchem-1125	234	60	)	)	PUNCT
eurjchem-1125	234	61	,	,	PUNCT
eurjchem-1125	234	62	288	288	NUM
eurjchem-1125	234	63	(	(	PUNCT
eurjchem-1125	234	64	4.4	4.4	NUM
eurjchem-1125	234	65	)	)	PUNCT
eurjchem-1125	234	66	,	,	PUNCT
eurjchem-1125	234	67	243	243	NUM
eurjchem-1125	234	68	(	(	PUNCT
eurjchem-1125	234	69	71.7	71.7	NUM
eurjchem-1125	234	70	)	)	PUNCT
eurjchem-1125	234	71	,	,	PUNCT
eurjchem-1125	234	72	225	225	NUM
eurjchem-1125	234	73	(	(	PUNCT
eurjchem-1125	234	74	81.1	81.1	NUM
eurjchem-1125	234	75	)	)	PUNCT
eurjchem-1125	234	76	,	,	PUNCT
eurjchem-1125	234	77	215	215	NUM
eurjchem-1125	234	78	(	(	PUNCT
eurjchem-1125	234	79	77.8	77.8	NUM
eurjchem-1125	234	80	)	)	PUNCT
eurjchem-1125	234	81	,	,	PUNCT
eurjchem-1125	234	82	178	178	NUM
eurjchem-1125	234	83	(	(	PUNCT
eurjchem-1125	234	84	100	100	NUM
eurjchem-1125	234	85	)	)	PUNCT
eurjchem-1125	234	86	,	,	PUNCT
eurjchem-1125	234	87	170	170	NUM
eurjchem-1125	234	88	(	(	PUNCT
eurjchem-1125	234	89	36.4	36.4	NUM
eurjchem-1125	234	90	)	)	PUNCT
eurjchem-1125	234	91	,	,	PUNCT
eurjchem-1125	234	92	150	150	NUM
eurjchem-1125	234	93	(	(	PUNCT
eurjchem-1125	234	94	66.9	66.9	NUM
eurjchem-1125	234	95	)	)	PUNCT
eurjchem-1125	234	96	,	,	PUNCT
eurjchem-1125	234	97	142	142	NUM
eurjchem-1125	234	98	(	(	PUNCT
eurjchem-1125	234	99	60.8	60.8	NUM
eurjchem-1125	234	100	)	)	PUNCT
eurjchem-1125	234	101	,	,	PUNCT
eurjchem-1125	234	102	122	122	NUM
eurjchem-1125	234	103	(	(	PUNCT
eurjchem-1125	234	104	49.4	49.4	NUM
eurjchem-1125	234	105	)	)	PUNCT
eurjchem-1125	234	106	,	,	PUNCT
eurjchem-1125	234	107	115	115	NUM
eurjchem-1125	234	108	(	(	PUNCT
eurjchem-1125	234	109	33.8	33.8	NUM
eurjchem-1125	234	110	)	)	PUNCT
eurjchem-1125	234	111	,	,	PUNCT
eurjchem-1125	234	112	90	90	NUM
eurjchem-1125	234	113	(	(	PUNCT
eurjchem-1125	234	114	31.9	31.9	NUM
eurjchem-1125	234	115	)	)	PUNCT
eurjchem-1125	234	116	,	,	PUNCT
eurjchem-1125	234	117	77	77	NUM
eurjchem-1125	234	118	(	(	PUNCT
eurjchem-1125	234	119	67.4	67.4	NUM
eurjchem-1125	234	120	)	)	PUNCT
eurjchem-1125	234	121	.	.	PUNCT
eurjchem-1125	235	1	anal	anal	PROPN
eurjchem-1125	235	2	.	.	PUNCT
eurjchem-1125	235	3	calcd	calcd	NOUN
eurjchem-1125	235	4	.	.	PUNCT
eurjchem-1125	236	1	for	for	SCONJ
eurjchem-1125	236	2	c25h27n3o5s2	c25h27n3o5s2	ADJ
eurjchem-1125	236	3	:	:	PUNCT
eurjchem-1125	236	4	c	c	X
eurjchem-1125	236	5	,	,	PUNCT
eurjchem-1125	236	6	58.46	58.46	NUM
eurjchem-1125	236	7	;	;	PUNCT
eurjchem-1125	236	8	h	h	NOUN
eurjchem-1125	236	9	,	,	PUNCT
eurjchem-1125	236	10	5.30	5.30	NUM
eurjchem-1125	236	11	;	;	PUNCT
eurjchem-1125	236	12	n	n	CCONJ
eurjchem-1125	236	13	,	,	PUNCT
eurjchem-1125	236	14	8.18	8.18	NUM
eurjchem-1125	236	15	.	.	PUNCT
eurjchem-1125	236	16	found	find	VERB
eurjchem-1125	236	17	:	:	PUNCT
eurjchem-1125	237	1	c	c	X
eurjchem-1125	237	2	,	,	PUNCT
eurjchem-1125	237	3	58.40	58.40	NUM
eurjchem-1125	237	4	;	;	PUNCT
eurjchem-1125	237	5	h	h	NOUN
eurjchem-1125	237	6	,	,	PUNCT
eurjchem-1125	237	7	5.36	5.36	NUM
eurjchem-1125	237	8	;	;	PUNCT
eurjchem-1125	237	9	n	n	CCONJ
eurjchem-1125	237	10	,	,	PUNCT
eurjchem-1125	237	11	8.13	8.13	NUM
eurjchem-1125	237	12	%	%	NOUN
eurjchem-1125	237	13	.	.	PUNCT
eurjchem-1125	238	1	2.3	2.3	NUM
eurjchem-1125	238	2	.	.	PUNCT
eurjchem-1125	239	1	antioxidant	antioxidant	NOUN
eurjchem-1125	239	2	screening	screen	VERB
eurjchem-1125	239	3	2.3.1	2.3.1	NUM
eurjchem-1125	239	4	.	.	PUNCT
eurjchem-1125	239	5	superoxide	superoxide	NOUN
eurjchem-1125	239	6	anion	anion	NOUN
eurjchem-1125	239	7	radical	radical	ADJ
eurjchem-1125	239	8	scavenging	scavenging	NOUN
eurjchem-1125	239	9	assay	assay	ADP
eurjchem-1125	239	10	the	the	DET
eurjchem-1125	239	11	assay	assay	NOUN
eurjchem-1125	239	12	was	be	AUX
eurjchem-1125	239	13	performed	perform	VERB
eurjchem-1125	239	14	according	accord	VERB
eurjchem-1125	239	15	to	to	ADP
eurjchem-1125	239	16	nishmiki	nishmiki	PROPN
eurjchem-1125	239	17	et	et	PROPN
eurjchem-1125	239	18	al	al	PROPN
eurjchem-1125	239	19	.	.	PUNCT
eurjchem-1125	240	1	[	[	X
eurjchem-1125	240	2	19	19	NUM
eurjchem-1125	240	3	]	]	PUNCT
eurjchem-1125	240	4	,	,	PUNCT
eurjchem-1125	240	5	with	with	ADP
eurjchem-1125	240	6	minor	minor	ADJ
eurjchem-1125	240	7	modifications	modification	NOUN
eurjchem-1125	240	8	.	.	PUNCT
eurjchem-1125	241	1	test	test	NOUN
eurjchem-1125	241	2	solution	solution	NOUN
eurjchem-1125	241	3	(	(	PUNCT
eurjchem-1125	241	4	0.1	0.1	NUM
eurjchem-1125	241	5	ml	ml	NOUN
eurjchem-1125	241	6	,	,	PUNCT
eurjchem-1125	241	7	1	1	NUM
eurjchem-1125	241	8	mg	mg	NUM
eurjchem-1125	241	9	/	/	SYM
eurjchem-1125	241	10	ml	ml	PROPN
eurjchem-1125	241	11	of	of	ADP
eurjchem-1125	241	12	sample	sample	NOUN
eurjchem-1125	241	13	solution	solution	NOUN
eurjchem-1125	241	14	(	(	PUNCT
eurjchem-1125	241	15	dmso	dmso	NOUN
eurjchem-1125	241	16	)	)	PUNCT
eurjchem-1125	241	17	)	)	PUNCT
eurjchem-1125	241	18	in	in	ADP
eurjchem-1125	241	19	0.1	0.1	NUM
eurjchem-1125	241	20	m	m	NOUN
eurjchem-1125	241	21	phosphate	phosphate	NOUN
eurjchem-1125	241	22	buffer	buffer	NOUN
eurjchem-1125	241	23	ph	ph	NOUN
eurjchem-1125	241	24	=	=	SYM
eurjchem-1125	241	25	7.4	7.4	NUM
eurjchem-1125	241	26	,	,	PUNCT
eurjchem-1125	241	27	62.5	62.5	NUM
eurjchem-1125	241	28	µl	µl	NOUN
eurjchem-1125	241	29	of	of	ADP
eurjchem-1125	241	30	468	468	NUM
eurjchem-1125	241	31	µm	µm	NOUN
eurjchem-1125	241	32	nadh	nadh	NOUN
eurjchem-1125	241	33	solution	solution	NOUN
eurjchem-1125	241	34	,	,	PUNCT
eurjchem-1125	241	35	62.5	62.5	NUM
eurjchem-1125	241	36	µl	µl	NOUN
eurjchem-1125	241	37	of	of	ADP
eurjchem-1125	241	38	156	156	NUM
eurjchem-1125	241	39	µm	µm	ADP
eurjchem-1125	241	40	nitroblue	nitroblue	PROPN
eurjchem-1125	241	41	tetrazolium	tetrazolium	NOUN
eurjchem-1125	241	42	(	(	PUNCT
eurjchem-1125	241	43	nbt	nbt	PROPN
eurjchem-1125	241	44	)	)	PUNCT
eurjchem-1125	241	45	solution	solution	NOUN
eurjchem-1125	241	46	and	and	CCONJ
eurjchem-1125	241	47	62.5	62.5	NUM
eurjchem-1125	241	48	µl	µl	NOUN
eurjchem-1125	241	49	of	of	ADP
eurjchem-1125	241	50	60	60	NUM
eurjchem-1125	241	51	µm	µm	ADP
eurjchem-1125	241	52	phenazine	phenazine	NOUN
eurjchem-1125	241	53	gouda	gouda	NOUN
eurjchem-1125	241	54	and	and	CCONJ
eurjchem-1125	241	55	el‐bialy	el‐bialy	PROPN
eurjchem-1125	241	56	/	/	SYM
eurjchem-1125	241	57	european	european	PROPN
eurjchem-1125	241	58	journal	journal	PROPN
eurjchem-1125	241	59	of	of	ADP
eurjchem-1125	241	60	chemistry	chemistry	NOUN
eurjchem-1125	241	61	5	5	NUM
eurjchem-1125	241	62	(	(	PUNCT
eurjchem-1125	241	63	4	4	NUM
eurjchem-1125	241	64	)	)	PUNCT
eurjchem-1125	241	65	(	(	PUNCT
eurjchem-1125	241	66	2014	2014	NUM
eurjchem-1125	241	67	)	)	PUNCT
eurjchem-1125	241	68	644‐651	644‐651	NUM
eurjchem-1125	241	69	649	649	NUM
eurjchem-1125	241	70	table	table	NOUN
eurjchem-1125	241	71	1	1	NUM
eurjchem-1125	241	72	.	.	X
eurjchem-1125	241	73	assay	assay	VERB
eurjchem-1125	241	74	for	for	ADP
eurjchem-1125	241	75	superoxide	superoxide	NOUN
eurjchem-1125	241	76	anion	anion	NOUN
eurjchem-1125	241	77	radical	radical	ADJ
eurjchem-1125	241	78	scavenging	scavenging	NOUN
eurjchem-1125	241	79	and	and	CCONJ
eurjchem-1125	241	80	bleomycin‐dependent	bleomycin‐dependent	NOUN
eurjchem-1125	241	81	dna	dna	NOUN
eurjchem-1125	241	82	damage	damage	NOUN
eurjchem-1125	241	83	(	(	PUNCT
eurjchem-1125	241	84	dna	dna	NOUN
eurjchem-1125	241	85	)	)	PUNCT
eurjchem-1125	241	86	compound	compound	NOUN
eurjchem-1125	241	87	no	no	DET
eurjchem-1125	241	88	antioxidant	antioxidant	ADJ
eurjchem-1125	241	89	activity	activity	NOUN
eurjchem-1125	241	90	(	(	PUNCT
eurjchem-1125	241	91	superoxide	superoxide	NOUN
eurjchem-1125	241	92	anion	anion	NOUN
eurjchem-1125	241	93	radical	radical	ADJ
eurjchem-1125	241	94	scavenging	scavenging	NOUN
eurjchem-1125	241	95	,	,	PUNCT
eurjchem-1125	241	96	%	%	INTJ
eurjchem-1125	241	97	)	)	PUNCT
eurjchem-1125	241	98	absorbance	absorbance	NOUN
eurjchem-1125	241	99	of	of	ADP
eurjchem-1125	241	100	samples	sample	NOUN
eurjchem-1125	241	101	ascorbic	ascorbic	NOUN
eurjchem-1125	241	102	acid	acid	NOUN
eurjchem-1125	241	103	66.1	66.1	NUM
eurjchem-1125	241	104	0.091	0.091	NUM
eurjchem-1125	241	105	1	1	NUM
eurjchem-1125	241	106	58.6	58.6	NUM
eurjchem-1125	241	107	0.078	0.078	NUM
eurjchem-1125	241	108	3	3	NUM
eurjchem-1125	241	109	48.6	48.6	NUM
eurjchem-1125	241	110	0.127	0.127	NUM
eurjchem-1125	241	111	4	4	NUM
eurjchem-1125	241	112	31.2	31.2	NUM
eurjchem-1125	241	113	0.080	0.080	NUM
eurjchem-1125	241	114	5	5	NUM
eurjchem-1125	241	115	35.7	35.7	NUM
eurjchem-1125	241	116	0.079	0.079	NUM
eurjchem-1125	241	117	6	6	NUM
eurjchem-1125	241	118	45.7	45.7	NUM
eurjchem-1125	241	119	0.113	0.113	NUM
eurjchem-1125	241	120	7	7	NUM
eurjchem-1125	241	121	61.4	61.4	NUM
eurjchem-1125	241	122	0.136	0.136	NUM
eurjchem-1125	241	123	8	8	NUM
eurjchem-1125	241	124	55.8	55.8	NUM
eurjchem-1125	241	125	0.125	0.125	NUM
eurjchem-1125	241	126	9	9	NUM
eurjchem-1125	241	127	41.4	41.4	NUM
eurjchem-1125	241	128	0.118	0.118	NUM
eurjchem-1125	241	129	10	10	NUM
eurjchem-1125	241	130	38.6	38.6	NUM
eurjchem-1125	241	131	0.157	0.157	NUM
eurjchem-1125	241	132	11	11	NUM
eurjchem-1125	241	133	10.3	10.3	NUM
eurjchem-1125	241	134	0.151	0.151	NUM
eurjchem-1125	241	135	12	12	NUM
eurjchem-1125	241	136	55.7	55.7	NUM
eurjchem-1125	241	137	0.102	0.102	NUM
eurjchem-1125	241	138	13	13	NUM
eurjchem-1125	241	139	6.1	6.1	NUM
eurjchem-1125	241	140	0.123	0.123	NUM
eurjchem-1125	241	141	14	14	NUM
eurjchem-1125	241	142	35.6	35.6	NUM
eurjchem-1125	241	143	0.145	0.145	NUM
eurjchem-1125	241	144	16	16	NUM
eurjchem-1125	241	145	58.9	58.9	NUM
eurjchem-1125	241	146	0.169	0.169	NUM
eurjchem-1125	241	147	17	17	NUM
eurjchem-1125	241	148	37.1	37.1	NUM
eurjchem-1125	241	149	0.134	0.134	NUM
eurjchem-1125	241	150	23	23	NUM
eurjchem-1125	241	151	57.1	57.1	NUM
eurjchem-1125	241	152	0.098	0.098	NUM
eurjchem-1125	241	153	24	24	NUM
eurjchem-1125	241	154	20.0	20.0	NUM
eurjchem-1125	241	155	0.100	0.100	NUM
eurjchem-1125	241	156	25	25	NUM
eurjchem-1125	241	157	18.6	18.6	NUM
eurjchem-1125	241	158	0.126	0.126	NUM
eurjchem-1125	241	159	*	*	PUNCT
eurjchem-1125	241	160	all	all	DET
eurjchem-1125	241	161	compounds	compound	NOUN
eurjchem-1125	241	162	were	be	AUX
eurjchem-1125	241	163	dissolved	dissolve	VERB
eurjchem-1125	241	164	in	in	ADP
eurjchem-1125	241	165	dmso	dmso	NOUN
eurjchem-1125	241	166	:	:	PUNCT
eurjchem-1125	241	167	meoh	meoh	PROPN
eurjchem-1125	241	168	(	(	PUNCT
eurjchem-1125	241	169	1:1	1:1	NUM
eurjchem-1125	241	170	,	,	PUNCT
eurjchem-1125	241	171	v	v	NOUN
eurjchem-1125	241	172	:	:	PUNCT
eurjchem-1125	241	173	v	v	NOUN
eurjchem-1125	241	174	)	)	PUNCT
eurjchem-1125	241	175	and	and	CCONJ
eurjchem-1125	241	176	tested	test	VERB
eurjchem-1125	241	177	at	at	ADP
eurjchem-1125	241	178	the	the	DET
eurjchem-1125	241	179	final	final	ADJ
eurjchem-1125	241	180	concentration	concentration	NOUN
eurjchem-1125	241	181	of	of	ADP
eurjchem-1125	241	182	0.1	0.1	NUM
eurjchem-1125	241	183	ml	ml	NOUN
eurjchem-1125	241	184	of	of	ADP
eurjchem-1125	241	185	1	1	NUM
eurjchem-1125	241	186	mg	mg	NUM
eurjchem-1125	241	187	/	/	SYM
eurjchem-1125	241	188	ml	ml	NOUN
eurjchem-1125	241	189	.	.	PUNCT
eurjchem-1125	242	1	scheme	scheme	NOUN
eurjchem-1125	242	2	5	5	NUM
eurjchem-1125	242	3	methophosphate	methophosphate	NOUN
eurjchem-1125	242	4	(	(	PUNCT
eurjchem-1125	242	5	pms	pms	NOUN
eurjchem-1125	242	6	)	)	PUNCT
eurjchem-1125	242	7	solution	solution	NOUN
eurjchem-1125	242	8	were	be	AUX
eurjchem-1125	242	9	added	add	VERB
eurjchem-1125	242	10	to	to	ADP
eurjchem-1125	242	11	a	a	DET
eurjchem-1125	242	12	microwell	microwell	NOUN
eurjchem-1125	242	13	plate	plate	NOUN
eurjchem-1125	242	14	and	and	CCONJ
eurjchem-1125	242	15	incubated	incubate	VERB
eurjchem-1125	242	16	at	at	ADP
eurjchem-1125	242	17	room	room	NOUN
eurjchem-1125	242	18	temperature	temperature	NOUN
eurjchem-1125	242	19	for	for	ADP
eurjchem-1125	242	20	5	5	NUM
eurjchem-1125	242	21	min	min	NOUN
eurjchem-1125	242	22	.	.	PROPN
eurjchem-1125	242	23	and	and	CCONJ
eurjchem-1125	242	24	the	the	DET
eurjchem-1125	242	25	abundance	abundance	NOUN
eurjchem-1125	242	26	at	at	ADP
eurjchem-1125	242	27	560	560	NUM
eurjchem-1125	242	28	nm	nm	NOUN
eurjchem-1125	242	29	was	be	AUX
eurjchem-1125	242	30	measured	measure	VERB
eurjchem-1125	242	31	against	against	ADP
eurjchem-1125	242	32	blank	blank	ADJ
eurjchem-1125	242	33	samples	sample	NOUN
eurjchem-1125	242	34	.	.	PUNCT
eurjchem-1125	243	1	the	the	DET
eurjchem-1125	243	2	capacity	capacity	NOUN
eurjchem-1125	243	3	of	of	ADP
eurjchem-1125	243	4	scavenging	scavenge	VERB
eurjchem-1125	243	5	super	super	ADJ
eurjchem-1125	243	6	oxide	oxide	NOUN
eurjchem-1125	243	7	radicals	radical	NOUN
eurjchem-1125	243	8	was	be	AUX
eurjchem-1125	243	9	calculated	calculate	VERB
eurjchem-1125	243	10	using	use	VERB
eurjchem-1125	243	11	the	the	DET
eurjchem-1125	243	12	following	follow	VERB
eurjchem-1125	243	13	formula	formula	NOUN
eurjchem-1125	243	14	:	:	PUNCT
eurjchem-1125	243	15	scavenging	scavenge	VERB
eurjchem-1125	243	16	activity	activity	NOUN
eurjchem-1125	243	17	=	=	PUNCT
eurjchem-1125	244	1	[	[	X
eurjchem-1125	244	2	a	a	DET
eurjchem-1125	244	3	(	(	PUNCT
eurjchem-1125	244	4	control	control	NOUN
eurjchem-1125	244	5	)	)	PUNCT
eurjchem-1125	244	6	‐	‐	ADP
eurjchem-1125	244	7	a	a	DET
eurjchem-1125	244	8	(	(	PUNCT
eurjchem-1125	244	9	test)/	test)/	NOUN
eurjchem-1125	244	10	a	a	DET
eurjchem-1125	244	11	(	(	PUNCT
eurjchem-1125	244	12	control	control	NOUN
eurjchem-1125	244	13	)	)	PUNCT
eurjchem-1125	244	14	]	]	PUNCT
eurjchem-1125	245	1	×	×	NOUN
eurjchem-1125	245	2	100	100	NUM
eurjchem-1125	245	3	(	(	PUNCT
eurjchem-1125	245	4	1	1	NUM
eurjchem-1125	245	5	)	)	PUNCT
eurjchem-1125	245	6	the	the	DET
eurjchem-1125	245	7	(	(	PUNCT
eurjchem-1125	245	8	nbt+nadh+pms	nbt+nadh+pm	NOUN
eurjchem-1125	245	9	)	)	PUNCT
eurjchem-1125	245	10	solution	solution	NOUN
eurjchem-1125	245	11	without	without	ADP
eurjchem-1125	245	12	sample	sample	NOUN
eurjchem-1125	245	13	solution	solution	NOUN
eurjchem-1125	245	14	was	be	AUX
eurjchem-1125	245	15	used	use	VERB
eurjchem-1125	245	16	as	as	ADP
eurjchem-1125	245	17	control	control	NOUN
eurjchem-1125	245	18	.	.	PUNCT
eurjchem-1125	246	1	2.3.2	2.3.2	NUM
eurjchem-1125	246	2	.	.	PUNCT
eurjchem-1125	246	3	bleomycin‐dependent	bleomycin‐dependent	PROPN
eurjchem-1125	246	4	dna	dna	PROPN
eurjchem-1125	246	5	damage	damage	NOUN
eurjchem-1125	246	6	the	the	DET
eurjchem-1125	246	7	assay	assay	NOUN
eurjchem-1125	246	8	was	be	AUX
eurjchem-1125	246	9	performed	perform	VERB
eurjchem-1125	246	10	according	accord	VERB
eurjchem-1125	246	11	to	to	ADP
eurjchem-1125	246	12	aeschlach	aeschlach	PROPN
eurjchem-1125	246	13	et	et	PROPN
eurjchem-1125	246	14	al	al	PROPN
eurjchem-1125	246	15	.	.	PUNCT
eurjchem-1125	247	1	[	[	X
eurjchem-1125	247	2	20	20	NUM
eurjchem-1125	247	3	]	]	PUNCT
eurjchem-1125	247	4	,	,	PUNCT
eurjchem-1125	247	5	with	with	ADP
eurjchem-1125	247	6	minor	minor	ADJ
eurjchem-1125	247	7	modifications	modification	NOUN
eurjchem-1125	247	8	.	.	PUNCT
eurjchem-1125	248	1	the	the	DET
eurjchem-1125	248	2	reaction	reaction	NOUN
eurjchem-1125	248	3	mixture	mixture	NOUN
eurjchem-1125	248	4	(	(	PUNCT
eurjchem-1125	248	5	0.5	0.5	NUM
eurjchem-1125	248	6	ml	ml	NOUN
eurjchem-1125	248	7	)	)	PUNCT
eurjchem-1125	248	8	contained	contain	VERB
eurjchem-1125	248	9	dna	dna	NOUN
eurjchem-1125	248	10	(	(	PUNCT
eurjchem-1125	248	11	0.5	0.5	NUM
eurjchem-1125	248	12	mg	mg	PROPN
eurjchem-1125	248	13	/	/	SYM
eurjchem-1125	248	14	ml	ml	NOUN
eurjchem-1125	248	15	)	)	PUNCT
eurjchem-1125	248	16	,	,	PUNCT
eurjchem-1125	248	17	bleomycin	bleomycin	PROPN
eurjchem-1125	248	18	sulfate	sulfate	NOUN
eurjchem-1125	248	19	(	(	PUNCT
eurjchem-1125	248	20	0.05	0.05	NUM
eurjchem-1125	248	21	mg	mg	NUM
eurjchem-1125	248	22	/	/	SYM
eurjchem-1125	248	23	ml	ml	NOUN
eurjchem-1125	248	24	)	)	PUNCT
eurjchem-1125	248	25	,	,	PUNCT
eurjchem-1125	248	26	mgcl2	mgcl2	PROPN
eurjchem-1125	249	1	(	(	PUNCT
eurjchem-1125	249	2	5	5	NUM
eurjchem-1125	249	3	mm	mm	NOUN
eurjchem-1125	249	4	)	)	PUNCT
eurjchem-1125	249	5	,	,	PUNCT
eurjchem-1125	249	6	fecl3	fecl3	PROPN
eurjchem-1125	250	1	(	(	PUNCT
eurjchem-1125	250	2	50	50	NUM
eurjchem-1125	250	3	mm	mm	NOUN
eurjchem-1125	250	4	)	)	PUNCT
eurjchem-1125	251	1	and	and	CCONJ
eurjchem-1125	251	2	samples	sample	NOUN
eurjchem-1125	251	3	to	to	PART
eurjchem-1125	251	4	be	be	AUX
eurjchem-1125	251	5	tested	test	VERB
eurjchem-1125	251	6	(	(	PUNCT
eurjchem-1125	251	7	0.1	0.1	NUM
eurjchem-1125	251	8	ml	ml	NOUN
eurjchem-1125	251	9	of	of	ADP
eurjchem-1125	251	10	1	1	NUM
eurjchem-1125	251	11	mg	mg	NUM
eurjchem-1125	251	12	/	/	SYM
eurjchem-1125	251	13	ml	ml	NOUN
eurjchem-1125	251	14	)	)	PUNCT
eurjchem-1125	251	15	.	.	PUNCT
eurjchem-1125	252	1	l‐ascorbic	l‐ascorbic	PROPN
eurjchem-1125	252	2	acid	acid	PROPN
eurjchem-1125	252	3	was	be	AUX
eurjchem-1125	252	4	used	use	VERB
eurjchem-1125	252	5	as	as	ADP
eurjchem-1125	252	6	a	a	DET
eurjchem-1125	252	7	positive	positive	ADJ
eurjchem-1125	252	8	control	control	NOUN
eurjchem-1125	252	9	.	.	PUNCT
eurjchem-1125	253	1	the	the	DET
eurjchem-1125	253	2	mixture	mixture	NOUN
eurjchem-1125	253	3	was	be	AUX
eurjchem-1125	253	4	incubated	incubate	VERB
eurjchem-1125	253	5	at	at	ADP
eurjchem-1125	253	6	37	37	NUM
eurjchem-1125	253	7	°	°	NOUN
eurjchem-1125	253	8	c	c	NOUN
eurjchem-1125	253	9	for	for	ADP
eurjchem-1125	253	10	1	1	NUM
eurjchem-1125	253	11	h.	h.	NOUN
eurjchem-1125	253	12	the	the	DET
eurjchem-1125	253	13	reaction	reaction	NOUN
eurjchem-1125	253	14	was	be	AUX
eurjchem-1125	253	15	terminated	terminate	VERB
eurjchem-1125	253	16	by	by	ADP
eurjchem-1125	253	17	addition	addition	NOUN
eurjchem-1125	253	18	of	of	ADP
eurjchem-1125	253	19	0.05	0.05	NUM
eurjchem-1125	253	20	ml	ml	NOUN
eurjchem-1125	253	21	edta	edta	NOUN
eurjchem-1125	253	22	(	(	PUNCT
eurjchem-1125	253	23	0.1	0.1	NUM
eurjchem-1125	253	24	m	m	NOUN
eurjchem-1125	253	25	)	)	PUNCT
eurjchem-1125	253	26	.	.	PUNCT
eurjchem-1125	254	1	the	the	DET
eurjchem-1125	254	2	color	color	NOUN
eurjchem-1125	254	3	was	be	AUX
eurjchem-1125	254	4	developed	develop	VERB
eurjchem-1125	254	5	by	by	ADP
eurjchem-1125	254	6	adding	add	VERB
eurjchem-1125	254	7	thiobarbituric	thiobarbituric	ADJ
eurjchem-1125	254	8	acid	acid	NOUN
eurjchem-1125	254	9	(	(	PUNCT
eurjchem-1125	254	10	tba	tba	NOUN
eurjchem-1125	254	11	)	)	PUNCT
eurjchem-1125	254	12	(	(	PUNCT
eurjchem-1125	254	13	0.5	0.5	NUM
eurjchem-1125	254	14	ml	ml	NOUN
eurjchem-1125	254	15	)	)	PUNCT
eurjchem-1125	254	16	(	(	PUNCT
eurjchem-1125	254	17	1	1	NUM
eurjchem-1125	254	18	%	%	NOUN
eurjchem-1125	254	19	,	,	PUNCT
eurjchem-1125	254	20	w	w	NOUN
eurjchem-1125	254	21	:	:	SYM
eurjchem-1125	254	22	v	v	NOUN
eurjchem-1125	254	23	)	)	PUNCT
eurjchem-1125	254	24	and	and	CCONJ
eurjchem-1125	254	25	hcl	hcl	PROPN
eurjchem-1125	254	26	(	(	PUNCT
eurjchem-1125	254	27	0.5	0.5	NUM
eurjchem-1125	254	28	ml	ml	NOUN
eurjchem-1125	254	29	)	)	PUNCT
eurjchem-1125	254	30	(	(	PUNCT
eurjchem-1125	254	31	25	25	NUM
eurjchem-1125	254	32	%	%	NOUN
eurjchem-1125	254	33	,	,	PUNCT
eurjchem-1125	254	34	v	v	NOUN
eurjchem-1125	254	35	:	:	PUNCT
eurjchem-1125	254	36	v	v	NOUN
eurjchem-1125	254	37	)	)	PUNCT
eurjchem-1125	254	38	followed	follow	VERB
eurjchem-1125	254	39	by	by	ADP
eurjchem-1125	254	40	heating	heat	VERB
eurjchem-1125	254	41	at	at	ADP
eurjchem-1125	254	42	80	80	NUM
eurjchem-1125	254	43	°	°	NUM
eurjchem-1125	254	44	c	c	NOUN
eurjchem-1125	254	45	for	for	ADP
eurjchem-1125	254	46	10	10	NUM
eurjchem-1125	254	47	min	min	NOUN
eurjchem-1125	254	48	.	.	PROPN
eurjchem-1125	255	1	after	after	ADP
eurjchem-1125	255	2	centrifugation	centrifugation	NOUN
eurjchem-1125	255	3	,	,	PUNCT
eurjchem-1125	255	4	the	the	DET
eurjchem-1125	255	5	extent	extent	NOUN
eurjchem-1125	255	6	of	of	ADP
eurjchem-1125	255	7	dna	dna	PROPN
eurjchem-1125	255	8	damage	damage	NOUN
eurjchem-1125	255	9	was	be	AUX
eurjchem-1125	255	10	measured	measure	VERB
eurjchem-1125	255	11	by	by	ADP
eurjchem-1125	255	12	the	the	DET
eurjchem-1125	255	13	increase	increase	NOUN
eurjchem-1125	255	14	in	in	ADP
eurjchem-1125	255	15	absorbance	absorbance	NOUN
eurjchem-1125	255	16	at	at	ADP
eurjchem-1125	255	17	532	532	NUM
eurjchem-1125	255	18	nm	nm	ADJ
eurjchem-1125	255	19	(	(	PUNCT
eurjchem-1125	255	20	table	table	NOUN
eurjchem-1125	255	21	1	1	NUM
eurjchem-1125	255	22	)	)	PUNCT
eurjchem-1125	255	23	.	.	PUNCT
eurjchem-1125	256	1	3	3	X
eurjchem-1125	256	2	.	.	NOUN
eurjchem-1125	256	3	results	result	NOUN
eurjchem-1125	256	4	and	and	CCONJ
eurjchem-1125	256	5	discussion	discussion	NOUN
eurjchem-1125	256	6	3.1	3.1	NUM
eurjchem-1125	256	7	.	.	PUNCT
eurjchem-1125	257	1	chemistry	chemistry	NOUN
eurjchem-1125	257	2	schemes	scheme	NOUN
eurjchem-1125	257	3	1‐4	1‐4	PRON
eurjchem-1125	257	4	describe	describe	VERB
eurjchem-1125	257	5	the	the	DET
eurjchem-1125	257	6	syntheses	synthesis	NOUN
eurjchem-1125	257	7	of	of	ADP
eurjchem-1125	257	8	the	the	DET
eurjchem-1125	257	9	target	target	NOUN
eurjchem-1125	257	10	molecules	molecule	NOUN
eurjchem-1125	257	11	.	.	PUNCT
eurjchem-1125	258	1	the	the	DET
eurjchem-1125	258	2	starting	start	VERB
eurjchem-1125	258	3	ethyl	ethyl	PROPN
eurjchem-1125	258	4	2‐[(cyanoacetyl)amino]‐4,5,6,7‐tetrahydro‐	2‐[(cyanoacetyl)amino]‐4,5,6,7‐tetrahydro‐	NUM
eurjchem-1125	259	1	1‐benzothiophene‐3‐carboxylate	1‐benzothiophene‐3‐carboxylate	NUM
eurjchem-1125	259	2	3	3	NUM
eurjchem-1125	259	3	[	[	X
eurjchem-1125	259	4	8	8	NUM
eurjchem-1125	259	5	]	]	PUNCT
eurjchem-1125	259	6	was	be	AUX
eurjchem-1125	259	7	prepared	prepare	VERB
eurjchem-1125	259	8	according	accord	VERB
eurjchem-1125	259	9	650	650	NUM
eurjchem-1125	259	10	gouda	gouda	NOUN
eurjchem-1125	259	11	and	and	CCONJ
eurjchem-1125	259	12	el‐bialy	el‐bialy	PROPN
eurjchem-1125	259	13	/	/	SYM
eurjchem-1125	259	14	european	european	PROPN
eurjchem-1125	259	15	journal	journal	PROPN
eurjchem-1125	259	16	of	of	ADP
eurjchem-1125	259	17	chemistry	chemistry	NOUN
eurjchem-1125	259	18	5	5	NUM
eurjchem-1125	259	19	(	(	PUNCT
eurjchem-1125	259	20	4	4	NUM
eurjchem-1125	259	21	)	)	PUNCT
eurjchem-1125	259	22	(	(	PUNCT
eurjchem-1125	259	23	2014	2014	NUM
eurjchem-1125	259	24	)	)	PUNCT
eurjchem-1125	259	25	644‐651	644‐651	NUM
eurjchem-1125	259	26	figure	figure	NOUN
eurjchem-1125	259	27	1	1	NUM
eurjchem-1125	259	28	.	.	PUNCT
eurjchem-1125	259	29	structure	structure	NOUN
eurjchem-1125	259	30	activity	activity	NOUN
eurjchem-1125	259	31	relationship	relationship	NOUN
eurjchem-1125	259	32	of	of	ADP
eurjchem-1125	259	33	the	the	DET
eurjchem-1125	259	34	more	more	ADV
eurjchem-1125	259	35	potent	potent	ADJ
eurjchem-1125	259	36	antioxidant	antioxidant	ADJ
eurjchem-1125	259	37	compounds	compound	NOUN
eurjchem-1125	259	38	.	.	PUNCT
eurjchem-1125	260	1	to	to	ADP
eurjchem-1125	260	2	the	the	DET
eurjchem-1125	260	3	previously	previously	ADV
eurjchem-1125	260	4	reported	report	VERB
eurjchem-1125	260	5	method	method	NOUN
eurjchem-1125	260	6	via	via	ADP
eurjchem-1125	260	7	refluxing	refluxing	NOUN
eurjchem-1125	260	8	of	of	ADP
eurjchem-1125	260	9	ethyl	ethyl	PROPN
eurjchem-1125	260	10	2‐	2‐	NUM
eurjchem-1125	260	11	amino‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxylate	amino‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxylate	PROPN
eurjchem-1125	260	12	(	(	PUNCT
eurjchem-1125	260	13	1	1	NUM
eurjchem-1125	260	14	)	)	PUNCT
eurjchem-1125	261	1	[	[	X
eurjchem-1125	261	2	17	17	NUM
eurjchem-1125	261	3	]	]	PUNCT
eurjchem-1125	261	4	with	with	ADP
eurjchem-1125	261	5	3‐(3,5‐dimethyl‐1h‐pyrazol‐1‐yl)‐3‐oxopropane	3‐(3,5‐dimethyl‐1h‐pyrazol‐1‐yl)‐3‐oxopropane	PROPN
eurjchem-1125	261	6	nitrile	nitrile	NOUN
eurjchem-1125	261	7	(	(	PUNCT
eurjchem-1125	261	8	2	2	NUM
eurjchem-1125	261	9	)	)	PUNCT
eurjchem-1125	262	1	[	[	X
eurjchem-1125	262	2	18	18	NUM
eurjchem-1125	262	3	]	]	PUNCT
eurjchem-1125	262	4	.	.	PUNCT
eurjchem-1125	263	1	multicomponent	multicomponent	NOUN
eurjchem-1125	263	2	condensation	condensation	NOUN
eurjchem-1125	263	3	of	of	ADP
eurjchem-1125	263	4	cyclopentanone	cyclopentanone	NOUN
eurjchem-1125	263	5	or	or	CCONJ
eurjchem-1125	263	6	cyclo	cyclo	NOUN
eurjchem-1125	263	7	hexanone	hexanone	NOUN
eurjchem-1125	263	8	with	with	ADP
eurjchem-1125	263	9	compound	compound	NOUN
eurjchem-1125	263	10	3	3	NUM
eurjchem-1125	263	11	and	and	CCONJ
eurjchem-1125	263	12	elemental	elemental	ADJ
eurjchem-1125	263	13	sulfur	sulfur	NOUN
eurjchem-1125	263	14	containing	contain	VERB
eurjchem-1125	263	15	morpholine	morpholine	NOUN
eurjchem-1125	263	16	as	as	ADP
eurjchem-1125	263	17	a	a	DET
eurjchem-1125	263	18	catalyst	catalyst	NOUN
eurjchem-1125	263	19	afforded	afford	VERB
eurjchem-1125	263	20	the	the	DET
eurjchem-1125	263	21	bithiophene	bithiophene	ADJ
eurjchem-1125	263	22	derivatives	derivative	NOUN
eurjchem-1125	263	23	4	4	NUM
eurjchem-1125	263	24	and	and	CCONJ
eurjchem-1125	263	25	5	5	NUM
eurjchem-1125	263	26	,	,	PUNCT
eurjchem-1125	263	27	respectively	respectively	ADV
eurjchem-1125	263	28	.	.	PUNCT
eurjchem-1125	264	1	compounds	compound	VERB
eurjchem-1125	264	2	4	4	NUM
eurjchem-1125	264	3	and	and	CCONJ
eurjchem-1125	264	4	5	5	NUM
eurjchem-1125	264	5	form	form	NOUN
eurjchem-1125	264	6	hydrogen	hydrogen	NOUN
eurjchem-1125	264	7	bonds	bond	NOUN
eurjchem-1125	264	8	between	between	ADP
eurjchem-1125	264	9	carbonyl	carbonyl	NOUN
eurjchem-1125	264	10	of	of	ADP
eurjchem-1125	264	11	esters	ester	NOUN
eurjchem-1125	264	12	and	and	CCONJ
eurjchem-1125	264	13	nh	nh	NOUN
eurjchem-1125	264	14	groups	group	NOUN
eurjchem-1125	264	15	of	of	ADP
eurjchem-1125	264	16	amide	amide	NOUN
eurjchem-1125	264	17	and	and	CCONJ
eurjchem-1125	264	18	between	between	ADP
eurjchem-1125	264	19	amino	amino	NOUN
eurjchem-1125	264	20	groups	group	NOUN
eurjchem-1125	264	21	and	and	CCONJ
eurjchem-1125	264	22	amidic	amidic	ADJ
eurjchem-1125	264	23	groups	group	NOUN
eurjchem-1125	264	24	.	.	PUNCT
eurjchem-1125	265	1	because	because	SCONJ
eurjchem-1125	265	2	the	the	DET
eurjchem-1125	265	3	ir	ir	PROPN
eurjchem-1125	265	4	spectra	spectra	PROPN
eurjchem-1125	265	5	revealed	reveal	VERB
eurjchem-1125	265	6	low	low	ADJ
eurjchem-1125	265	7	stretching	stretching	NOUN
eurjchem-1125	265	8	vibrations	vibration	NOUN
eurjchem-1125	265	9	of	of	ADP
eurjchem-1125	265	10	ester	ester	NOUN
eurjchem-1125	265	11	and	and	CCONJ
eurjchem-1125	265	12	amidic	amidic	ADJ
eurjchem-1125	265	13	carbonyl	carbonyl	NOUN
eurjchem-1125	265	14	groups	group	NOUN
eurjchem-1125	265	15	and	and	CCONJ
eurjchem-1125	265	16	the	the	DET
eurjchem-1125	265	17	1h	1h	NUM
eurjchem-1125	265	18	nmr	nmr	NOUN
eurjchem-1125	265	19	spectra	spectra	NOUN
eurjchem-1125	265	20	show	show	VERB
eurjchem-1125	265	21	the	the	DET
eurjchem-1125	265	22	presence	presence	NOUN
eurjchem-1125	265	23	of	of	ADP
eurjchem-1125	265	24	nh	nh	PROPN
eurjchem-1125	265	25	singlet	singlet	NOUN
eurjchem-1125	265	26	signal	signal	NOUN
eurjchem-1125	265	27	at	at	ADP
eurjchem-1125	265	28	11.04	11.04	NUM
eurjchem-1125	265	29	and	and	CCONJ
eurjchem-1125	265	30	11.10	11.10	NUM
eurjchem-1125	265	31	ppm	ppm	NOUN
eurjchem-1125	265	32	,	,	PUNCT
eurjchem-1125	265	33	respectively	respectively	ADV
eurjchem-1125	265	34	,	,	PUNCT
eurjchem-1125	265	35	similar	similar	ADJ
eurjchem-1125	265	36	behaviour	behaviour	NOUN
eurjchem-1125	265	37	was	be	AUX
eurjchem-1125	265	38	reported	report	VERB
eurjchem-1125	265	39	[	[	X
eurjchem-1125	265	40	21	21	NUM
eurjchem-1125	265	41	]	]	PUNCT
eurjchem-1125	265	42	.	.	PUNCT
eurjchem-1125	266	1	moreover	moreover	ADV
eurjchem-1125	266	2	,	,	PUNCT
eurjchem-1125	266	3	cyanoacetylation	cyanoacetylation	NOUN
eurjchem-1125	266	4	of	of	ADP
eurjchem-1125	266	5	compound	compound	NOUN
eurjchem-1125	266	6	4	4	NUM
eurjchem-1125	266	7	and	and	CCONJ
eurjchem-1125	266	8	5	5	NUM
eurjchem-1125	266	9	under	under	ADP
eurjchem-1125	266	10	the	the	DET
eurjchem-1125	266	11	same	same	ADJ
eurjchem-1125	266	12	previous	previous	ADJ
eurjchem-1125	266	13	conditions	condition	NOUN
eurjchem-1125	266	14	afforded	afford	VERB
eurjchem-1125	266	15	the	the	DET
eurjchem-1125	266	16	cyanoacetamide	cyanoacetamide	ADJ
eurjchem-1125	266	17	derivatives	derivative	NOUN
eurjchem-1125	266	18	6	6	NUM
eurjchem-1125	266	19	and	and	CCONJ
eurjchem-1125	266	20	7	7	NUM
eurjchem-1125	266	21	.	.	X
eurjchem-1125	266	22	treatment	treatment	NOUN
eurjchem-1125	266	23	of	of	ADP
eurjchem-1125	266	24	compound	compound	NOUN
eurjchem-1125	266	25	7	7	NUM
eurjchem-1125	266	26	with	with	ADP
eurjchem-1125	266	27	cyclopentanone	cyclopentanone	NOUN
eurjchem-1125	266	28	or	or	CCONJ
eurjchem-1125	266	29	cyclohexanone	cyclohexanone	ADJ
eurjchem-1125	266	30	and	and	CCONJ
eurjchem-1125	266	31	elemental	elemental	ADJ
eurjchem-1125	266	32	sulfur	sulfur	NOUN
eurjchem-1125	266	33	in	in	ADP
eurjchem-1125	266	34	ethanol	ethanol	NOUN
eurjchem-1125	266	35	containing	contain	VERB
eurjchem-1125	266	36	morpholine	morpholine	NOUN
eurjchem-1125	266	37	afforded	afford	VERB
eurjchem-1125	266	38	the	the	DET
eurjchem-1125	266	39	corresponding	corresponding	ADJ
eurjchem-1125	266	40	trithiophene	trithiophene	NOUN
eurjchem-1125	266	41	derivatives	derivative	NOUN
eurjchem-1125	266	42	8	8	NUM
eurjchem-1125	266	43	and	and	CCONJ
eurjchem-1125	266	44	9	9	NUM
eurjchem-1125	266	45	,	,	PUNCT
eurjchem-1125	266	46	respectively	respectively	ADV
eurjchem-1125	266	47	.	.	PUNCT
eurjchem-1125	267	1	compound	compound	NOUN
eurjchem-1125	267	2	8	8	NUM
eurjchem-1125	267	3	and	and	CCONJ
eurjchem-1125	267	4	9	9	NUM
eurjchem-1125	267	5	formed	form	VERB
eurjchem-1125	267	6	three	three	NUM
eurjchem-1125	267	7	hydrogen	hydrogen	NOUN
eurjchem-1125	267	8	bonds	bond	NOUN
eurjchem-1125	267	9	(	(	PUNCT
eurjchem-1125	267	10	scheme	scheme	NOUN
eurjchem-1125	267	11	1	1	NUM
eurjchem-1125	267	12	)	)	PUNCT
eurjchem-1125	267	13	.	.	PUNCT
eurjchem-1125	268	1	knoevenagel	knoevenagel	NOUN
eurjchem-1125	268	2	condensation	condensation	NOUN
eurjchem-1125	268	3	of	of	ADP
eurjchem-1125	268	4	compound	compound	NOUN
eurjchem-1125	268	5	7	7	NUM
eurjchem-1125	268	6	with	with	ADP
eurjchem-1125	268	7	4‐n	4‐n	NUM
eurjchem-1125	268	8	,	,	PUNCT
eurjchem-1125	268	9	n‐	n‐	NOUN
eurjchem-1125	268	10	dimethylaminobezaldehyde	dimethylaminobezaldehyde	NOUN
eurjchem-1125	268	11	,	,	PUNCT
eurjchem-1125	268	12	4‐piperdin‐1‐ylbenzaldehyde	4‐piperdin‐1‐ylbenzaldehyde	NUM
eurjchem-1125	268	13	or	or	CCONJ
eurjchem-1125	268	14	salicyaldehyde	salicyaldehyde	NOUN
eurjchem-1125	268	15	in	in	ADP
eurjchem-1125	268	16	ethanol	ethanol	NOUN
eurjchem-1125	268	17	containing	contain	VERB
eurjchem-1125	268	18	a	a	DET
eurjchem-1125	268	19	catalytic	catalytic	ADJ
eurjchem-1125	268	20	amount	amount	NOUN
eurjchem-1125	268	21	of	of	ADP
eurjchem-1125	268	22	piperidine	piperidine	NOUN
eurjchem-1125	268	23	afforded	afford	VERB
eurjchem-1125	268	24	the	the	DET
eurjchem-1125	268	25	corresponding	correspond	VERB
eurjchem-1125	268	26	(	(	PUNCT
eurjchem-1125	268	27	e	e	NOUN
eurjchem-1125	268	28	)	)	PUNCT
eurjchem-1125	268	29	arylidenes	arylidene	NOUN
eurjchem-1125	268	30	10	10	NUM
eurjchem-1125	268	31	,	,	PUNCT
eurjchem-1125	268	32	11	11	NUM
eurjchem-1125	268	33	and	and	CCONJ
eurjchem-1125	268	34	coumarin	coumarin	VERB
eurjchem-1125	268	35	derivative	derivative	ADJ
eurjchem-1125	268	36	12	12	NUM
eurjchem-1125	268	37	,	,	PUNCT
eurjchem-1125	268	38	respectively	respectively	ADV
eurjchem-1125	268	39	[	[	X
eurjchem-1125	268	40	22	22	NUM
eurjchem-1125	268	41	]	]	PUNCT
eurjchem-1125	268	42	(	(	PUNCT
eurjchem-1125	268	43	scheme	scheme	NOUN
eurjchem-1125	268	44	2	2	NUM
eurjchem-1125	268	45	)	)	PUNCT
eurjchem-1125	268	46	.	.	PUNCT
eurjchem-1125	269	1	furthermore	furthermore	ADV
eurjchem-1125	269	2	,	,	PUNCT
eurjchem-1125	269	3	condensation	condensation	NOUN
eurjchem-1125	269	4	of	of	ADP
eurjchem-1125	269	5	compound	compound	NOUN
eurjchem-1125	269	6	3	3	NUM
eurjchem-1125	269	7	with	with	ADP
eurjchem-1125	269	8	terphthaldehyde	terphthaldehyde	NOUN
eurjchem-1125	269	9	in	in	ADP
eurjchem-1125	269	10	ethanol	ethanol	NOUN
eurjchem-1125	269	11	containing	contain	VERB
eurjchem-1125	269	12	a	a	DET
eurjchem-1125	269	13	catalytic	catalytic	ADJ
eurjchem-1125	269	14	amount	amount	NOUN
eurjchem-1125	269	15	of	of	ADP
eurjchem-1125	269	16	piperidine	piperidine	NOUN
eurjchem-1125	269	17	achieved	achieve	VERB
eurjchem-1125	269	18	the	the	DET
eurjchem-1125	269	19	(	(	PUNCT
eurjchem-1125	269	20	e	e	NOUN
eurjchem-1125	269	21	)	)	PUNCT
eurjchem-1125	269	22	bis‐arylidene	bis‐arylidene	NOUN
eurjchem-1125	269	23	derivative	derivative	ADJ
eurjchem-1125	269	24	13	13	NUM
eurjchem-1125	270	1	[	[	X
eurjchem-1125	270	2	23	23	NUM
eurjchem-1125	270	3	]	]	PUNCT
eurjchem-1125	270	4	.	.	PUNCT
eurjchem-1125	271	1	coupling	couple	VERB
eurjchem-1125	271	2	of	of	ADP
eurjchem-1125	271	3	compound	compound	NOUN
eurjchem-1125	271	4	3	3	NUM
eurjchem-1125	271	5	with	with	ADP
eurjchem-1125	271	6	benzene‐1,4‐bis(diazonium	benzene‐1,4‐bis(diazonium	NOUN
eurjchem-1125	271	7	)	)	PUNCT
eurjchem-1125	271	8	dichloride	dichloride	PROPN
eurjchem-1125	271	9	afforded	afford	VERB
eurjchem-1125	271	10	the	the	DET
eurjchem-1125	271	11	(	(	PUNCT
eurjchem-1125	271	12	e	e	NOUN
eurjchem-1125	271	13	)	)	PUNCT
eurjchem-1125	271	14	hydrazo	hydrazo	NOUN
eurjchem-1125	271	15	derivative	derivative	ADJ
eurjchem-1125	271	16	14	14	NUM
eurjchem-1125	272	1	[	[	X
eurjchem-1125	272	2	21	21	NUM
eurjchem-1125	272	3	]	]	X
eurjchem-1125	272	4	(	(	PUNCT
eurjchem-1125	272	5	bioisostere	bioisostere	NOUN
eurjchem-1125	272	6	of	of	ADP
eurjchem-1125	272	7	compound	compound	NOUN
eurjchem-1125	272	8	13	13	NUM
eurjchem-1125	272	9	)	)	PUNCT
eurjchem-1125	272	10	(	(	PUNCT
eurjchem-1125	272	11	scheme	scheme	NOUN
eurjchem-1125	272	12	3	3	NUM
eurjchem-1125	272	13	)	)	PUNCT
eurjchem-1125	272	14	.	.	PUNCT
eurjchem-1125	273	1	on	on	ADP
eurjchem-1125	273	2	the	the	DET
eurjchem-1125	273	3	other	other	ADJ
eurjchem-1125	273	4	hand	hand	NOUN
eurjchem-1125	273	5	,	,	PUNCT
eurjchem-1125	273	6	stirring	stirring	NOUN
eurjchem-1125	273	7	of	of	ADP
eurjchem-1125	273	8	compound	compound	NOUN
eurjchem-1125	273	9	3	3	NUM
eurjchem-1125	273	10	with	with	ADP
eurjchem-1125	273	11	carbon	carbon	NOUN
eurjchem-1125	273	12	disulphide	disulphide	ADV
eurjchem-1125	273	13	in	in	ADP
eurjchem-1125	273	14	dmf	dmf	PROPN
eurjchem-1125	273	15	containing	contain	VERB
eurjchem-1125	273	16	potassium	potassium	NOUN
eurjchem-1125	273	17	hydroxide	hydroxide	NOUN
eurjchem-1125	273	18	followed	follow	VERB
eurjchem-1125	273	19	by	by	ADP
eurjchem-1125	273	20	in	in	ADP
eurjchem-1125	273	21	situ	situ	ADJ
eurjchem-1125	273	22	addition	addition	NOUN
eurjchem-1125	273	23	of	of	ADP
eurjchem-1125	273	24	ethyl	ethyl	PROPN
eurjchem-1125	273	25	bromoacetate	bromoacetate	NOUN
eurjchem-1125	273	26	afforded	afford	VERB
eurjchem-1125	273	27	the	the	DET
eurjchem-1125	273	28	triester	triester	NOUN
eurjchem-1125	273	29	derivative	derivative	ADJ
eurjchem-1125	273	30	16	16	NUM
eurjchem-1125	273	31	via	via	ADP
eurjchem-1125	273	32	the	the	DET
eurjchem-1125	273	33	intermediate	intermediate	ADJ
eurjchem-1125	273	34	15	15	NUM
eurjchem-1125	273	35	,	,	PUNCT
eurjchem-1125	273	36	which	which	PRON
eurjchem-1125	273	37	afforded	afford	VERB
eurjchem-1125	273	38	the	the	DET
eurjchem-1125	273	39	dithiophene	dithiophene	NOUN
eurjchem-1125	273	40	17	17	NUM
eurjchem-1125	273	41	upon	upon	SCONJ
eurjchem-1125	273	42	heating	heating	NOUN
eurjchem-1125	273	43	in	in	ADP
eurjchem-1125	273	44	dmf	dmf	PROPN
eurjchem-1125	273	45	containing	contain	VERB
eurjchem-1125	273	46	a	a	DET
eurjchem-1125	273	47	catalytic	catalytic	ADJ
eurjchem-1125	273	48	amount	amount	NOUN
eurjchem-1125	273	49	of	of	ADP
eurjchem-1125	273	50	triethylamine	triethylamine	NOUN
eurjchem-1125	273	51	(	(	PUNCT
eurjchem-1125	273	52	scheme	scheme	NOUN
eurjchem-1125	273	53	4	4	NUM
eurjchem-1125	273	54	)	)	PUNCT
eurjchem-1125	273	55	.	.	PUNCT
eurjchem-1125	274	1	attempting	attempt	VERB
eurjchem-1125	274	2	for	for	ADP
eurjchem-1125	274	3	preparation	preparation	NOUN
eurjchem-1125	274	4	of	of	ADP
eurjchem-1125	274	5	compounds	compound	NOUN
eurjchem-1125	274	6	21	21	NUM
eurjchem-1125	274	7	and	and	CCONJ
eurjchem-1125	274	8	22	22	NUM
eurjchem-1125	274	9	,	,	PUNCT
eurjchem-1125	274	10	which	which	PRON
eurjchem-1125	274	11	were	be	AUX
eurjchem-1125	274	12	bioisostere	bioisostere	NUM
eurjchem-1125	274	13	of	of	ADP
eurjchem-1125	274	14	compound	compound	NOUN
eurjchem-1125	274	15	16	16	NUM
eurjchem-1125	274	16	via	via	ADP
eurjchem-1125	274	17	reaction	reaction	NOUN
eurjchem-1125	274	18	of	of	ADP
eurjchem-1125	274	19	compound	compound	NOUN
eurjchem-1125	274	20	3	3	NUM
eurjchem-1125	274	21	with	with	ADP
eurjchem-1125	274	22	phenyl	phenyl	NOUN
eurjchem-1125	274	23	isothiocyanate	isothiocyanate	NOUN
eurjchem-1125	274	24	in	in	ADP
eurjchem-1125	274	25	dry	dry	PROPN
eurjchem-1125	274	26	dmf	dmf	PROPN
eurjchem-1125	274	27	in	in	ADP
eurjchem-1125	274	28	the	the	DET
eurjchem-1125	274	29	presence	presence	NOUN
eurjchem-1125	274	30	of	of	ADP
eurjchem-1125	274	31	potassium	potassium	NOUN
eurjchem-1125	274	32	hydroxide	hydroxide	NOUN
eurjchem-1125	274	33	followed	follow	VERB
eurjchem-1125	274	34	by	by	ADP
eurjchem-1125	274	35	addition	addition	NOUN
eurjchem-1125	274	36	of	of	ADP
eurjchem-1125	274	37	reaction	reaction	NOUN
eurjchem-1125	274	38	with	with	ADP
eurjchem-1125	274	39	chloroacetone	chloroacetone	PROPN
eurjchem-1125	274	40	or	or	CCONJ
eurjchem-1125	274	41	ethyl	ethyl	PROPN
eurjchem-1125	274	42	bromoacetate	bromoacetate	NOUN
eurjchem-1125	274	43	was	be	AUX
eurjchem-1125	274	44	failed	fail	VERB
eurjchem-1125	274	45	.	.	PUNCT
eurjchem-1125	275	1	although	although	SCONJ
eurjchem-1125	275	2	both	both	PRON
eurjchem-1125	275	3	compound	compound	VERB
eurjchem-1125	275	4	21	21	NUM
eurjchem-1125	275	5	and	and	CCONJ
eurjchem-1125	275	6	22	22	NUM
eurjchem-1125	275	7	were	be	AUX
eurjchem-1125	275	8	formed	form	VERB
eurjchem-1125	275	9	in	in	ADP
eurjchem-1125	275	10	situ	situ	NOUN
eurjchem-1125	275	11	,	,	PUNCT
eurjchem-1125	275	12	subsequently	subsequently	ADV
eurjchem-1125	275	13	cyclized	cyclize	VERB
eurjchem-1125	275	14	to	to	ADP
eurjchem-1125	275	15	the	the	DET
eurjchem-1125	275	16	2‐{[(2z)‐2‐cyano‐2‐(4‐methyl‐3‐	2‐{[(2z)‐2‐cyano‐2‐(4‐methyl‐3‐	NUM
eurjchem-1125	275	17	phenyl‐1,3‐thiazol‐2(3h)‐ylidene)acetyl]amino}‐4,5,6,7‐tetra	phenyl‐1,3‐thiazol‐2(3h)‐ylidene)acetyl]amino}‐4,5,6,7‐tetra	PROPN
eurjchem-1125	275	18	hydro‐1‐benzothiophene‐3‐carboxylate	hydro‐1‐benzothiophene‐3‐carboxylate	NOUN
eurjchem-1125	275	19	(	(	PUNCT
eurjchem-1125	275	20	19	19	NUM
eurjchem-1125	275	21	)	)	PUNCT
eurjchem-1125	275	22	and	and	CCONJ
eurjchem-1125	275	23	ethyl	ethyl	PROPN
eurjchem-1125	275	24	2‐{[(2z	2‐{[(2z	NUM
eurjchem-1125	275	25	)	)	PUNCT
eurjchem-1125	275	26	‐2‐cyano‐2‐(4‐oxo‐3‐phenyl‐1,3‐thiazolidin‐2‐ylidene)acetyl	‐2‐cyano‐2‐(4‐oxo‐3‐phenyl‐1,3‐thiazolidin‐2‐ylidene)acetyl	PROPN
eurjchem-1125	275	27	]	]	X
eurjchem-1125	275	28	amino}‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxylate	amino}‐4,5,6,7‐tetrahydro‐1‐benzothiophene‐3‐carboxylate	NUM
eurjchem-1125	275	29	(	(	PUNCT
eurjchem-1125	275	30	20	20	NUM
eurjchem-1125	275	31	)	)	PUNCT
eurjchem-1125	275	32	,	,	PUNCT
eurjchem-1125	275	33	respectively	respectively	ADV
eurjchem-1125	275	34	[	[	X
eurjchem-1125	275	35	8	8	NUM
eurjchem-1125	275	36	]	]	SYM
eurjchem-1125	275	37	.	.	PUNCT
eurjchem-1125	276	1	acidification	acidification	NOUN
eurjchem-1125	276	2	of	of	ADP
eurjchem-1125	276	3	the	the	DET
eurjchem-1125	276	4	intermediate	intermediate	ADJ
eurjchem-1125	276	5	potassium	potassium	NOUN
eurjchem-1125	276	6	salt	salt	NOUN
eurjchem-1125	276	7	15	15	NUM
eurjchem-1125	276	8	afforded	afford	VERB
eurjchem-1125	276	9	compound	compound	NOUN
eurjchem-1125	276	10	23	23	NUM
eurjchem-1125	277	1	[	[	X
eurjchem-1125	277	2	8	8	NUM
eurjchem-1125	277	3	]	]	PUNCT
eurjchem-1125	277	4	,	,	PUNCT
eurjchem-1125	277	5	refluxing	refluxing	NOUN
eurjchem-1125	277	6	of	of	ADP
eurjchem-1125	277	7	compound	compound	NOUN
eurjchem-1125	277	8	23	23	NUM
eurjchem-1125	277	9	with	with	ADP
eurjchem-1125	277	10	chloroacetone	chloroacetone	NOUN
eurjchem-1125	277	11	or	or	CCONJ
eurjchem-1125	277	12	ethyl	ethyl	PROPN
eurjchem-1125	277	13	bromoacetate	bromoacetate	NOUN
eurjchem-1125	277	14	afforded	afford	VERB
eurjchem-1125	277	15	the	the	DET
eurjchem-1125	277	16	dithiophene	dithiophene	NOUN
eurjchem-1125	277	17	derivatives	derivative	NOUN
eurjchem-1125	277	18	24	24	NUM
eurjchem-1125	277	19	and	and	CCONJ
eurjchem-1125	277	20	25	25	NUM
eurjchem-1125	277	21	(	(	PUNCT
eurjchem-1125	277	22	bioisoster	bioisoster	NOUN
eurjchem-1125	277	23	of	of	ADP
eurjchem-1125	277	24	compound	compound	NOUN
eurjchem-1125	277	25	17	17	NUM
eurjchem-1125	277	26	)	)	PUNCT
eurjchem-1125	277	27	,	,	PUNCT
eurjchem-1125	277	28	respectively	respectively	ADV
eurjchem-1125	277	29	(	(	PUNCT
eurjchem-1125	277	30	scheme	scheme	NOUN
eurjchem-1125	277	31	5	5	NUM
eurjchem-1125	277	32	)	)	PUNCT
eurjchem-1125	277	33	.	.	PUNCT
eurjchem-1125	278	1	the	the	DET
eurjchem-1125	278	2	structure	structure	NOUN
eurjchem-1125	278	3	of	of	ADP
eurjchem-1125	278	4	new	new	ADJ
eurjchem-1125	278	5	synthesized	synthesize	VERB
eurjchem-1125	278	6	compounds	compound	NOUN
eurjchem-1125	278	7	was	be	AUX
eurjchem-1125	278	8	established	establish	VERB
eurjchem-1125	278	9	on	on	ADP
eurjchem-1125	278	10	the	the	DET
eurjchem-1125	278	11	basis	basis	NOUN
eurjchem-1125	278	12	of	of	ADP
eurjchem-1125	278	13	their	their	PRON
eurjchem-1125	278	14	elemental	elemental	ADJ
eurjchem-1125	278	15	analyses	analysis	NOUN
eurjchem-1125	278	16	and	and	CCONJ
eurjchem-1125	278	17	spectral	spectral	ADJ
eurjchem-1125	278	18	data	datum	NOUN
eurjchem-1125	278	19	(	(	PUNCT
eurjchem-1125	278	20	ir	ir	PROPN
eurjchem-1125	278	21	,	,	PUNCT
eurjchem-1125	278	22	1h	1h	NUM
eurjchem-1125	278	23	,	,	PUNCT
eurjchem-1125	278	24	13c	13c	NOUN
eurjchem-1125	278	25	nmr	nmr	NOUN
eurjchem-1125	278	26	and	and	CCONJ
eurjchem-1125	278	27	mass	mass	ADJ
eurjchem-1125	278	28	spectral	spectral	ADJ
eurjchem-1125	278	29	data	data	PROPN
eurjchem-1125	278	30	,	,	PUNCT
eurjchem-1125	278	31	c.f	c.f	PROPN
eurjchem-1125	278	32	.	.	PROPN
eurjchem-1125	278	33	experimental	experimental	ADJ
eurjchem-1125	278	34	section	section	NOUN
eurjchem-1125	278	35	)	)	PUNCT
eurjchem-1125	278	36	.	.	PUNCT
eurjchem-1125	279	1	3.2	3.2	NUM
eurjchem-1125	279	2	.	.	PUNCT
eurjchem-1125	280	1	biological	biological	ADJ
eurjchem-1125	280	2	assays	assay	NOUN
eurjchem-1125	280	3	3.2.1	3.2.1	NUM
eurjchem-1125	280	4	.	.	PUNCT
eurjchem-1125	280	5	superoxide	superoxide	NOUN
eurjchem-1125	280	6	anion	anion	NOUN
eurjchem-1125	280	7	radical	radical	ADJ
eurjchem-1125	280	8	scavenging	scavenging	NOUN
eurjchem-1125	280	9	assay	assay	VERB
eurjchem-1125	280	10	the	the	DET
eurjchem-1125	280	11	antioxidant	antioxidant	ADJ
eurjchem-1125	280	12	activity	activity	NOUN
eurjchem-1125	280	13	of	of	ADP
eurjchem-1125	280	14	the	the	DET
eurjchem-1125	280	15	new	new	ADJ
eurjchem-1125	280	16	synthesized	synthesize	VERB
eurjchem-1125	280	17	compounds	compound	NOUN
eurjchem-1125	280	18	was	be	AUX
eurjchem-1125	280	19	evaluated	evaluate	VERB
eurjchem-1125	280	20	following	follow	VERB
eurjchem-1125	280	21	the	the	DET
eurjchem-1125	280	22	protocols	protocol	NOUN
eurjchem-1125	280	23	published	publish	VERB
eurjchem-1125	280	24	by	by	ADP
eurjchem-1125	280	25	nishimiki	nishimiki	PROPN
eurjchem-1125	280	26	et	et	PROPN
eurjchem-1125	280	27	al	al	PROPN
eurjchem-1125	280	28	.	.	PUNCT
eurjchem-1125	281	1	[	[	X
eurjchem-1125	281	2	19	19	NUM
eurjchem-1125	281	3	]	]	PUNCT
eurjchem-1125	281	4	.	.	PUNCT
eurjchem-1125	282	1	the	the	DET
eurjchem-1125	282	2	biological	biological	ADJ
eurjchem-1125	282	3	data	datum	NOUN
eurjchem-1125	282	4	showed	show	VERB
eurjchem-1125	282	5	clearly	clearly	ADV
eurjchem-1125	282	6	that	that	SCONJ
eurjchem-1125	282	7	compounds	compound	VERB
eurjchem-1125	282	8	1	1	NUM
eurjchem-1125	282	9	,	,	PUNCT
eurjchem-1125	282	10	7	7	NUM
eurjchem-1125	282	11	,	,	PUNCT
eurjchem-1125	282	12	8	8	NUM
eurjchem-1125	282	13	,	,	PUNCT
eurjchem-1125	282	14	12	12	NUM
eurjchem-1125	282	15	,	,	PUNCT
eurjchem-1125	282	16	16	16	NUM
eurjchem-1125	282	17	and	and	CCONJ
eurjchem-1125	282	18	23	23	NUM
eurjchem-1125	282	19	have	have	VERB
eurjchem-1125	282	20	good	good	ADJ
eurjchem-1125	282	21	activities	activity	NOUN
eurjchem-1125	282	22	,	,	PUNCT
eurjchem-1125	282	23	while	while	SCONJ
eurjchem-1125	282	24	compounds	compound	NOUN
eurjchem-1125	282	25	3‐6	3‐6	NUM
eurjchem-1125	282	26	,	,	PUNCT
eurjchem-1125	282	27	9	9	NUM
eurjchem-1125	282	28	,	,	PUNCT
eurjchem-1125	282	29	10	10	NUM
eurjchem-1125	282	30	,	,	PUNCT
eurjchem-1125	282	31	14	14	NUM
eurjchem-1125	282	32	and	and	CCONJ
eurjchem-1125	282	33	17	17	NUM
eurjchem-1125	282	34	exhibited	exhibit	VERB
eurjchem-1125	282	35	moderate	moderate	ADJ
eurjchem-1125	282	36	activities	activity	NOUN
eurjchem-1125	282	37	.	.	PUNCT
eurjchem-1125	283	1	on	on	ADP
eurjchem-1125	283	2	the	the	DET
eurjchem-1125	283	3	other	other	ADJ
eurjchem-1125	283	4	hand	hand	NOUN
eurjchem-1125	283	5	,	,	PUNCT
eurjchem-1125	283	6	the	the	DET
eurjchem-1125	283	7	anther	anther	NOUN
eurjchem-1125	283	8	compounds	compound	NOUN
eurjchem-1125	283	9	exhibited	exhibit	VERB
eurjchem-1125	283	10	weak	weak	ADJ
eurjchem-1125	283	11	activities	activity	NOUN
eurjchem-1125	283	12	(	(	PUNCT
eurjchem-1125	283	13	table	table	NOUN
eurjchem-1125	283	14	1	1	NUM
eurjchem-1125	283	15	)	)	PUNCT
eurjchem-1125	283	16	.	.	PUNCT
eurjchem-1125	284	1	thus	thus	ADV
eurjchem-1125	284	2	,	,	PUNCT
eurjchem-1125	284	3	it	it	PRON
eurjchem-1125	284	4	would	would	AUX
eurjchem-1125	284	5	appear	appear	VERB
eurjchem-1125	284	6	that	that	SCONJ
eurjchem-1125	284	7	introducing	introduce	VERB
eurjchem-1125	284	8	of	of	ADP
eurjchem-1125	284	9	cyanoacetamide	cyanoacetamide	ADJ
eurjchem-1125	284	10	,	,	PUNCT
eurjchem-1125	284	11	thiocarbamoyl	thiocarbamoyl	NOUN
eurjchem-1125	284	12	,	,	PUNCT
eurjchem-1125	284	13	thiophene	thiophene	NOUN
eurjchem-1125	284	14	and	and	CCONJ
eurjchem-1125	284	15	coumarin	coumarin	NOUN
eurjchem-1125	284	16	moieties	moiety	NOUN
eurjchem-1125	284	17	enhances	enhance	VERB
eurjchem-1125	284	18	the	the	DET
eurjchem-1125	284	19	antioxidant	antioxidant	ADJ
eurjchem-1125	284	20	properties	property	NOUN
eurjchem-1125	284	21	of	of	ADP
eurjchem-1125	284	22	2‐aminothiophene	2‐aminothiophene	NUM
eurjchem-1125	284	23	derivatives	derivative	NOUN
eurjchem-1125	284	24	.	.	PUNCT
eurjchem-1125	285	1	all	all	DET
eurjchem-1125	285	2	compounds	compound	NOUN
eurjchem-1125	285	3	were	be	AUX
eurjchem-1125	285	4	dissolved	dissolve	VERB
eurjchem-1125	285	5	in	in	ADP
eurjchem-1125	285	6	dmso	dmso	NOUN
eurjchem-1125	285	7	:	:	PUNCT
eurjchem-1125	285	8	meoh	meoh	PROPN
eurjchem-1125	285	9	(	(	PUNCT
eurjchem-1125	285	10	1:1	1:1	NUM
eurjchem-1125	285	11	,	,	PUNCT
eurjchem-1125	285	12	v	v	NOUN
eurjchem-1125	285	13	:	:	PUNCT
eurjchem-1125	285	14	v	v	NOUN
eurjchem-1125	285	15	)	)	PUNCT
eurjchem-1125	285	16	and	and	CCONJ
eurjchem-1125	285	17	tested	test	VERB
eurjchem-1125	285	18	at	at	ADP
eurjchem-1125	285	19	the	the	DET
eurjchem-1125	285	20	final	final	ADJ
eurjchem-1125	285	21	concentration	concentration	NOUN
eurjchem-1125	285	22	of	of	ADP
eurjchem-1125	285	23	0.1	0.1	NUM
eurjchem-1125	285	24	ml	ml	NOUN
eurjchem-1125	285	25	of	of	ADP
eurjchem-1125	285	26	1	1	NUM
eurjchem-1125	285	27	mg	mg	NUM
eurjchem-1125	285	28	/	/	SYM
eurjchem-1125	285	29	ml	ml	NOUN
eurjchem-1125	285	30	.	.	PUNCT
eurjchem-1125	286	1	the	the	DET
eurjchem-1125	286	2	extent	extent	NOUN
eurjchem-1125	286	3	of	of	ADP
eurjchem-1125	286	4	dna	dna	PROPN
eurjchem-1125	286	5	damage	damage	NOUN
eurjchem-1125	286	6	is	be	AUX
eurjchem-1125	286	7	expressed	express	VERB
eurjchem-1125	286	8	by	by	ADP
eurjchem-1125	286	9	increase	increase	NOUN
eurjchem-1125	286	10	of	of	ADP
eurjchem-1125	286	11	absorbance	absorbance	NOUN
eurjchem-1125	286	12	at	at	ADP
eurjchem-1125	286	13	520	520	NUM
eurjchem-1125	286	14	nm	nm	NOUN
eurjchem-1125	286	15	.	.	PUNCT
eurjchem-1125	287	1	the	the	DET
eurjchem-1125	287	2	synthesized	synthesize	VERB
eurjchem-1125	287	3	compounds	compound	NOUN
eurjchem-1125	287	4	were	be	AUX
eurjchem-1125	287	5	test	test	NOUN
eurjchem-1125	287	6	for	for	ADP
eurjchem-1125	287	7	bleomycin‐dependent	bleomycin‐dependent	NOUN
eurjchem-1125	287	8	dna	dna	PROPN
eurjchem-1125	287	9	damage	damage	NOUN
eurjchem-1125	287	10	(	(	PUNCT
eurjchem-1125	287	11	table	table	NOUN
eurjchem-1125	287	12	1	1	NUM
eurjchem-1125	287	13	)	)	PUNCT
eurjchem-1125	287	14	and	and	CCONJ
eurjchem-1125	287	15	showed	show	VERB
eurjchem-1125	287	16	that	that	SCONJ
eurjchem-1125	287	17	compounds	compound	NOUN
eurjchem-1125	287	18	1	1	NUM
eurjchem-1125	287	19	,	,	PUNCT
eurjchem-1125	287	20	4	4	NUM
eurjchem-1125	287	21	,	,	PUNCT
eurjchem-1125	287	22	5	5	NUM
eurjchem-1125	287	23	,	,	PUNCT
eurjchem-1125	287	24	12	12	NUM
eurjchem-1125	287	25	,	,	PUNCT
eurjchem-1125	287	26	23	23	NUM
eurjchem-1125	287	27	and	and	CCONJ
eurjchem-1125	287	28	24	24	NUM
eurjchem-1125	287	29	have	have	VERB
eurjchem-1125	287	30	an	an	DET
eurjchem-1125	287	31	ability	ability	NOUN
eurjchem-1125	287	32	to	to	PART
eurjchem-1125	287	33	protect	protect	VERB
eurjchem-1125	287	34	dna	dna	NOUN
eurjchem-1125	287	35	from	from	ADP
eurjchem-1125	287	36	the	the	DET
eurjchem-1125	287	37	induced	induced	ADJ
eurjchem-1125	287	38	damage	damage	NOUN
eurjchem-1125	287	39	by	by	ADP
eurjchem-1125	287	40	bleomycin	bleomycin	PROPN
eurjchem-1125	287	41	.	.	PUNCT
eurjchem-1125	288	1	by	by	ADP
eurjchem-1125	288	2	comparing	compare	VERB
eurjchem-1125	288	3	the	the	DET
eurjchem-1125	288	4	results	result	NOUN
eurjchem-1125	288	5	obtained	obtain	VERB
eurjchem-1125	288	6	of	of	ADP
eurjchem-1125	288	7	antioxidant	antioxidant	NOUN
eurjchem-1125	288	8	of	of	ADP
eurjchem-1125	288	9	the	the	DET
eurjchem-1125	288	10	compounds	compound	NOUN
eurjchem-1125	288	11	reported	report	VERB
eurjchem-1125	288	12	in	in	ADP
eurjchem-1125	288	13	this	this	DET
eurjchem-1125	288	14	paper	paper	NOUN
eurjchem-1125	288	15	to	to	ADP
eurjchem-1125	288	16	their	their	PRON
eurjchem-1125	288	17	structures	structure	NOUN
eurjchem-1125	288	18	,	,	PUNCT
eurjchem-1125	288	19	the	the	DET
eurjchem-1125	288	20	following	follow	VERB
eurjchem-1125	288	21	structure	structure	NOUN
eurjchem-1125	288	22	activity	activity	NOUN
eurjchem-1125	288	23	relationship	relationship	NOUN
eurjchem-1125	288	24	(	(	PUNCT
eurjchem-1125	288	25	sar	sar	PROPN
eurjchem-1125	288	26	's	's	PART
eurjchem-1125	288	27	)	)	PUNCT
eurjchem-1125	288	28	were	be	AUX
eurjchem-1125	288	29	postulated	postulate	VERB
eurjchem-1125	288	30	:	:	PUNCT
eurjchem-1125	288	31	(	(	PUNCT
eurjchem-1125	288	32	i	i	NOUN
eurjchem-1125	288	33	)	)	PUNCT
eurjchem-1125	289	1	2‐aminothiophene	2‐aminothiophene	NUM
eurjchem-1125	289	2	derivatives	derivative	NOUN
eurjchem-1125	289	3	1	1	NUM
eurjchem-1125	289	4	,	,	PUNCT
eurjchem-1125	289	5	4	4	NUM
eurjchem-1125	289	6	and	and	CCONJ
eurjchem-1125	289	7	5	5	NUM
eurjchem-1125	289	8	are	be	AUX
eurjchem-1125	289	9	more	more	ADV
eurjchem-1125	289	10	potent	potent	ADJ
eurjchem-1125	289	11	than	than	ADP
eurjchem-1125	289	12	ascorbic	ascorbic	NOUN
eurjchem-1125	289	13	acid	acid	NOUN
eurjchem-1125	289	14	which	which	PRON
eurjchem-1125	289	15	may	may	AUX
eurjchem-1125	289	16	be	be	AUX
eurjchem-1125	289	17	attributed	attribute	VERB
eurjchem-1125	289	18	to	to	ADP
eurjchem-1125	289	19	the	the	DET
eurjchem-1125	289	20	replacement	replacement	NOUN
eurjchem-1125	289	21	of	of	ADP
eurjchem-1125	289	22	furan	furan	PROPN
eurjchem-1125	289	23	moiety	moiety	PROPN
eurjchem-1125	289	24	with	with	ADP
eurjchem-1125	289	25	the	the	DET
eurjchem-1125	289	26	thiophene	thiophene	NOUN
eurjchem-1125	289	27	moiety	moiety	NOUN
eurjchem-1125	289	28	and	and	CCONJ
eurjchem-1125	289	29	presence	presence	NOUN
eurjchem-1125	289	30	of	of	ADP
eurjchem-1125	289	31	amino	amino	NOUN
eurjchem-1125	289	32	group	group	NOUN
eurjchem-1125	289	33	.	.	PUNCT
eurjchem-1125	290	1	(	(	PUNCT
eurjchem-1125	290	2	ii	ii	NOUN
eurjchem-1125	290	3	)	)	PUNCT
eurjchem-1125	290	4	compounds	compound	VERB
eurjchem-1125	290	5	3	3	NUM
eurjchem-1125	290	6	,	,	PUNCT
eurjchem-1125	290	7	6	6	NUM
eurjchem-1125	290	8	and	and	CCONJ
eurjchem-1125	290	9	7	7	NUM
eurjchem-1125	290	10	(	(	PUNCT
eurjchem-1125	290	11	n‐substituted‐2‐amino	n‐substituted‐2‐amino	NOUN
eurjchem-1125	290	12	thiophene	thiophene	NOUN
eurjchem-1125	290	13	)	)	PUNCT
eurjchem-1125	290	14	is	be	AUX
eurjchem-1125	290	15	less	less	ADV
eurjchem-1125	290	16	potent	potent	ADJ
eurjchem-1125	290	17	than	than	ADP
eurjchem-1125	290	18	compounds	compound	NOUN
eurjchem-1125	290	19	1	1	NUM
eurjchem-1125	290	20	,	,	PUNCT
eurjchem-1125	290	21	4	4	NUM
eurjchem-1125	290	22	and	and	CCONJ
eurjchem-1125	290	23	5	5	NUM
eurjchem-1125	290	24	,	,	PUNCT
eurjchem-1125	290	25	gouda	gouda	NOUN
eurjchem-1125	290	26	and	and	CCONJ
eurjchem-1125	290	27	el‐bialy	el‐bialy	PROPN
eurjchem-1125	290	28	/	/	SYM
eurjchem-1125	290	29	european	european	PROPN
eurjchem-1125	290	30	journal	journal	PROPN
eurjchem-1125	290	31	of	of	ADP
eurjchem-1125	290	32	chemistry	chemistry	NOUN
eurjchem-1125	290	33	5	5	NUM
eurjchem-1125	290	34	(	(	PUNCT
eurjchem-1125	290	35	4	4	NUM
eurjchem-1125	290	36	)	)	PUNCT
eurjchem-1125	290	37	(	(	PUNCT
eurjchem-1125	290	38	2014	2014	NUM
eurjchem-1125	290	39	)	)	PUNCT
eurjchem-1125	291	1	644‐651	644‐651	NUM
eurjchem-1125	291	2	651	651	NUM
eurjchem-1125	291	3	respectively	respectively	ADV
eurjchem-1125	291	4	which	which	PRON
eurjchem-1125	291	5	may	may	AUX
eurjchem-1125	291	6	be	be	AUX
eurjchem-1125	291	7	due	due	ADJ
eurjchem-1125	291	8	to	to	PART
eurjchem-1125	291	9	decrease	decrease	NOUN
eurjchem-1125	291	10	of	of	ADP
eurjchem-1125	291	11	basicity	basicity	NOUN
eurjchem-1125	291	12	of	of	ADP
eurjchem-1125	291	13	amino	amino	NOUN
eurjchem-1125	291	14	group	group	NOUN
eurjchem-1125	291	15	.	.	PUNCT
eurjchem-1125	292	1	(	(	PUNCT
eurjchem-1125	292	2	iii	iii	X
eurjchem-1125	292	3	)	)	PUNCT
eurjchem-1125	292	4	sulfanyl	sulfanyl	VERB
eurjchem-1125	292	5	derivative	derivative	ADJ
eurjchem-1125	292	6	23	23	NUM
eurjchem-1125	292	7	is	be	AUX
eurjchem-1125	292	8	more	more	ADV
eurjchem-1125	292	9	potent	potent	ADJ
eurjchem-1125	292	10	than	than	ADP
eurjchem-1125	292	11	3	3	NUM
eurjchem-1125	292	12	which	which	PRON
eurjchem-1125	292	13	may	may	AUX
eurjchem-1125	292	14	be	be	AUX
eurjchem-1125	292	15	attributable	attributable	ADJ
eurjchem-1125	292	16	to	to	ADP
eurjchem-1125	292	17	presence	presence	NOUN
eurjchem-1125	292	18	of	of	ADP
eurjchem-1125	292	19	thiocarbamoyl	thiocarbamoyl	PROPN
eurjchem-1125	292	20	moiety	moiety	NOUN
eurjchem-1125	292	21	or	or	CCONJ
eurjchem-1125	292	22	may	may	AUX
eurjchem-1125	292	23	be	be	AUX
eurjchem-1125	292	24	due	due	ADJ
eurjchem-1125	292	25	to	to	ADP
eurjchem-1125	292	26	oxidation	oxidation	NOUN
eurjchem-1125	292	27	of	of	ADP
eurjchem-1125	292	28	s‐h	s‐h	PROPN
eurjchem-1125	292	29	to	to	ADP
eurjchem-1125	292	30	s‐s	s‐s	PROPN
eurjchem-1125	292	31	and	and	CCONJ
eurjchem-1125	292	32	presence	presence	NOUN
eurjchem-1125	292	33	of	of	ADP
eurjchem-1125	292	34	further	further	ADJ
eurjchem-1125	292	35	conjugation	conjugation	NOUN
eurjchem-1125	292	36	.	.	PUNCT
eurjchem-1125	293	1	(	(	PUNCT
eurjchem-1125	293	2	iv	iv	X
eurjchem-1125	293	3	)	)	PUNCT
eurjchem-1125	293	4	compounds	compound	VERB
eurjchem-1125	293	5	12	12	NUM
eurjchem-1125	293	6	and	and	CCONJ
eurjchem-1125	293	7	24	24	NUM
eurjchem-1125	293	8	exhibited	exhibit	VERB
eurjchem-1125	293	9	high	high	ADJ
eurjchem-1125	293	10	antioxidant	antioxidant	ADJ
eurjchem-1125	293	11	activity	activity	NOUN
eurjchem-1125	293	12	which	which	PRON
eurjchem-1125	293	13	may	may	AUX
eurjchem-1125	293	14	be	be	AUX
eurjchem-1125	293	15	due	due	ADJ
eurjchem-1125	293	16	presence	presence	NOUN
eurjchem-1125	293	17	of	of	ADP
eurjchem-1125	293	18	imino	imino	NOUN
eurjchem-1125	293	19	coumarin	coumarin	NOUN
eurjchem-1125	293	20	and	and	CCONJ
eurjchem-1125	293	21	3‐aminothiophene	3‐aminothiophene	NUM
eurjchem-1125	293	22	moiety	moiety	NOUN
eurjchem-1125	293	23	(	(	PUNCT
eurjchem-1125	293	24	figure	figure	NOUN
eurjchem-1125	293	25	1	1	NUM
eurjchem-1125	293	26	)	)	PUNCT
eurjchem-1125	293	27	.	.	PUNCT
eurjchem-1125	294	1	4	4	X
eurjchem-1125	294	2	.	.	X
eurjchem-1125	294	3	conclusion	conclusion	VERB
eurjchem-1125	294	4	the	the	DET
eurjchem-1125	294	5	objective	objective	NOUN
eurjchem-1125	294	6	of	of	ADP
eurjchem-1125	294	7	the	the	DET
eurjchem-1125	294	8	present	present	ADJ
eurjchem-1125	294	9	study	study	NOUN
eurjchem-1125	294	10	was	be	AUX
eurjchem-1125	294	11	to	to	PART
eurjchem-1125	294	12	synthesize	synthesize	VERB
eurjchem-1125	294	13	and	and	CCONJ
eurjchem-1125	294	14	evaluate	evaluate	VERB
eurjchem-1125	294	15	the	the	DET
eurjchem-1125	294	16	antioxidant	antioxidant	ADJ
eurjchem-1125	294	17	activity	activity	NOUN
eurjchem-1125	294	18	of	of	ADP
eurjchem-1125	294	19	some	some	DET
eurjchem-1125	294	20	novel	novel	ADJ
eurjchem-1125	294	21	bis‐thiophenes	bis‐thiophene	NOUN
eurjchem-1125	294	22	with	with	ADP
eurjchem-1125	294	23	the	the	DET
eurjchem-1125	294	24	hope	hope	NOUN
eurjchem-1125	294	25	of	of	ADP
eurjchem-1125	294	26	discovering	discover	VERB
eurjchem-1125	294	27	new	new	ADJ
eurjchem-1125	294	28	structure	structure	NOUN
eurjchem-1125	294	29	leads	lead	VERB
eurjchem-1125	294	30	serving	serve	VERB
eurjchem-1125	294	31	as	as	ADP
eurjchem-1125	294	32	antioxidant	antioxidant	ADJ
eurjchem-1125	294	33	agents	agent	NOUN
eurjchem-1125	294	34	.	.	PUNCT
eurjchem-1125	295	1	the	the	DET
eurjchem-1125	295	2	data	datum	NOUN
eurjchem-1125	295	3	clearly	clearly	ADV
eurjchem-1125	295	4	showed	show	VERB
eurjchem-1125	295	5	that	that	SCONJ
eurjchem-1125	295	6	compounds	compound	NOUN
eurjchem-1125	295	7	1	1	NUM
eurjchem-1125	295	8	,	,	PUNCT
eurjchem-1125	295	9	7	7	NUM
eurjchem-1125	295	10	,	,	PUNCT
eurjchem-1125	295	11	8	8	NUM
eurjchem-1125	295	12	,	,	PUNCT
eurjchem-1125	295	13	12	12	NUM
eurjchem-1125	295	14	,	,	PUNCT
eurjchem-1125	295	15	16	16	NUM
eurjchem-1125	295	16	and	and	CCONJ
eurjchem-1125	295	17	23	23	NUM
eurjchem-1125	295	18	have	have	VERB
eurjchem-1125	295	19	good	good	ADJ
eurjchem-1125	295	20	activities	activity	NOUN
eurjchem-1125	295	21	exhibited	exhibit	VERB
eurjchem-1125	295	22	weak	weak	ADJ
eurjchem-1125	295	23	anti‐	anti‐	NOUN
eurjchem-1125	295	24	oxidant	oxidant	ADJ
eurjchem-1125	295	25	activities	activity	NOUN
eurjchem-1125	295	26	by	by	ADP
eurjchem-1125	295	27	superoxide	superoxide	NOUN
eurjchem-1125	295	28	anion	anion	NOUN
eurjchem-1125	295	29	radical	radical	ADJ
eurjchem-1125	295	30	scavenging	scavenging	NOUN
eurjchem-1125	295	31	assay	assay	NOUN
eurjchem-1125	295	32	.	.	PUNCT
eurjchem-1125	296	1	on	on	ADP
eurjchem-1125	296	2	the	the	DET
eurjchem-1125	296	3	other	other	ADJ
eurjchem-1125	296	4	hand	hand	NOUN
eurjchem-1125	296	5	,	,	PUNCT
eurjchem-1125	296	6	compounds	compound	VERB
eurjchem-1125	296	7	1	1	NUM
eurjchem-1125	296	8	,	,	PUNCT
eurjchem-1125	296	9	4	4	NUM
eurjchem-1125	296	10	,	,	PUNCT
eurjchem-1125	296	11	5	5	NUM
eurjchem-1125	296	12	,	,	PUNCT
eurjchem-1125	296	13	12	12	NUM
eurjchem-1125	296	14	,	,	PUNCT
eurjchem-1125	296	15	23	23	NUM
eurjchem-1125	296	16	and	and	CCONJ
eurjchem-1125	296	17	24	24	NUM
eurjchem-1125	296	18	have	have	VERB
eurjchem-1125	296	19	an	an	DET
eurjchem-1125	296	20	ability	ability	NOUN
eurjchem-1125	296	21	to	to	PART
eurjchem-1125	296	22	protect	protect	VERB
eurjchem-1125	296	23	dna	dna	NOUN
eurjchem-1125	296	24	from	from	ADP
eurjchem-1125	296	25	the	the	DET
eurjchem-1125	296	26	induced	induced	ADJ
eurjchem-1125	296	27	damage	damage	NOUN
eurjchem-1125	296	28	by	by	ADP
eurjchem-1125	296	29	bleomycin	bleomycin	PROPN
eurjchem-1125	296	30	.	.	PUNCT
eurjchem-1125	297	1	acknowledgements	acknowledgement	NOUN
eurjchem-1125	297	2	we	we	PRON
eurjchem-1125	297	3	deeply	deeply	ADV
eurjchem-1125	297	4	appreciate	appreciate	VERB
eurjchem-1125	297	5	the	the	DET
eurjchem-1125	297	6	assistance	assistance	NOUN
eurjchem-1125	297	7	of	of	ADP
eurjchem-1125	297	8	dr	dr	PROPN
eurjchem-1125	297	9	.	.	PROPN
eurjchem-1125	297	10	ahmed	ahmed	PROPN
eurjchem-1125	297	11	abass	abass	PROPN
eurjchem-1125	297	12	,	,	PUNCT
eurjchem-1125	297	13	pharmacognosy	pharmacognosy	PROPN
eurjchem-1125	297	14	department	department	NOUN
eurjchem-1125	297	15	,	,	PUNCT
eurjchem-1125	297	16	faculty	faculty	NOUN
eurjchem-1125	297	17	of	of	ADP
eurjchem-1125	297	18	pharmacy	pharmacy	NOUN
eurjchem-1125	297	19	,	,	PUNCT
eurjchem-1125	297	20	mansoura	mansoura	PROPN
eurjchem-1125	297	21	university	university	NOUN
eurjchem-1125	297	22	,	,	PUNCT
eurjchem-1125	297	23	mansoura	mansoura	PROPN
eurjchem-1125	297	24	,	,	PUNCT
eurjchem-1125	297	25	egypt	egypt	PROPN
eurjchem-1125	297	26	for	for	ADP
eurjchem-1125	297	27	screening	screening	NOUN
eurjchem-1125	297	28	of	of	ADP
eurjchem-1125	297	29	the	the	DET
eurjchem-1125	297	30	biological	biological	ADJ
eurjchem-1125	297	31	activities	activity	NOUN
eurjchem-1125	297	32	of	of	ADP
eurjchem-1125	297	33	the	the	DET
eurjchem-1125	297	34	tested	test	VERB
eurjchem-1125	297	35	compounds	compound	NOUN
eurjchem-1125	297	36	references	reference	NOUN
eurjchem-1125	297	37	[	[	X
eurjchem-1125	297	38	1	1	NUM
eurjchem-1125	297	39	]	]	PUNCT
eurjchem-1125	297	40	.	.	PUNCT
eurjchem-1125	298	1	lutjens	lutjen	NOUN
eurjchem-1125	298	2	,	,	PUNCT
eurjchem-1125	298	3	h.	h.	NOUN
eurjchem-1125	298	4	;	;	PUNCT
eurjchem-1125	298	5	zickgraft	zickgraft	NOUN
eurjchem-1125	298	6	,	,	PUNCT
eurjchem-1125	298	7	a.	a.	NOUN
eurjchem-1125	298	8	;	;	PUNCT
eurjchem-1125	298	9	figler	figler	PROPN
eurjchem-1125	298	10	,	,	PUNCT
eurjchem-1125	298	11	h.	h.	PROPN
eurjchem-1125	298	12	;	;	PUNCT
eurjchem-1125	298	13	linden	linden	PROPN
eurjchem-1125	298	14	,	,	PUNCT
eurjchem-1125	298	15	j.	j.	PROPN
eurjchem-1125	298	16	;	;	PUNCT
eurjchem-1125	298	17	olsson	olsson	PROPN
eurjchem-1125	298	18	,	,	PUNCT
eurjchem-1125	298	19	r.	r.	PROPN
eurjchem-1125	298	20	a.	a.	PROPN
eurjchem-1125	298	21	;	;	PUNCT
eurjchem-1125	298	22	scammels	scammel	NOUN
eurjchem-1125	298	23	,	,	PUNCT
eurjchem-1125	298	24	p.	p.	PROPN
eurjchem-1125	298	25	j.	j.	PROPN
eurjchem-1125	298	26	j.	j.	PROPN
eurjchem-1125	298	27	med	med	PROPN
eurjchem-1125	298	28	.	.	PROPN
eurjchem-1125	298	29	chem	chem	PROPN
eurjchem-1125	298	30	.	.	PUNCT
eurjchem-1125	299	1	2003	2003	NUM
eurjchem-1125	299	2	,	,	PUNCT
eurjchem-1125	299	3	46	46	NUM
eurjchem-1125	299	4	,	,	PUNCT
eurjchem-1125	299	5	1870‐1877	1870‐1877	NOUN
eurjchem-1125	299	6	.	.	PUNCT
eurjchem-1125	300	1	[	[	X
eurjchem-1125	300	2	2	2	NUM
eurjchem-1125	300	3	]	]	PUNCT
eurjchem-1125	300	4	.	.	PUNCT
eurjchem-1125	301	1	nikolakopoulos	nikolakopoulos	PROPN
eurjchem-1125	301	2	,	,	PUNCT
eurjchem-1125	301	3	g.	g.	PROPN
eurjchem-1125	301	4	;	;	PUNCT
eurjchem-1125	301	5	figler	figler	PROPN
eurjchem-1125	301	6	,	,	PUNCT
eurjchem-1125	301	7	h.	h.	PROPN
eurjchem-1125	301	8	;	;	PUNCT
eurjchem-1125	301	9	linden	linden	PROPN
eurjchem-1125	301	10	,	,	PUNCT
eurjchem-1125	301	11	j.	j.	PROPN
eurjchem-1125	301	12	;	;	PUNCT
eurjchem-1125	301	13	scammels	scammel	VERB
eurjchem-1125	301	14	p.	p.	PROPN
eurjchem-1125	301	15	j.	j.	PROPN
eurjchem-1125	301	16	bioorg	bioorg	PROPN
eurjchem-1125	301	17	.	.	PUNCT
eurjchem-1125	302	1	med	med	PROPN
eurjchem-1125	302	2	.	.	PROPN
eurjchem-1125	302	3	chem	chem	PROPN
eurjchem-1125	302	4	.	.	PUNCT
eurjchem-1125	303	1	2006	2006	NUM
eurjchem-1125	303	2	,	,	PUNCT
eurjchem-1125	303	3	14	14	NUM
eurjchem-1125	303	4	,	,	PUNCT
eurjchem-1125	303	5	2358‐2365	2358‐2365	NUM
eurjchem-1125	303	6	.	.	PUNCT
eurjchem-1125	304	1	[	[	X
eurjchem-1125	304	2	3	3	NUM
eurjchem-1125	304	3	]	]	PUNCT
eurjchem-1125	304	4	.	.	PUNCT
eurjchem-1125	305	1	pillai	pillai	PROPN
eurjchem-1125	305	2	,	,	PUNCT
eurjchem-1125	305	3	a.	a.	PROPN
eurjchem-1125	305	4	d.	d.	PROPN
eurjchem-1125	305	5	;	;	PUNCT
eurjchem-1125	305	6	rani	rani	PROPN
eurjchem-1125	305	7	,	,	PUNCT
eurjchem-1125	305	8	s.	s.	PROPN
eurjchem-1125	305	9	;	;	PUNCT
eurjchem-1125	305	10	rathod	rathod	PROPN
eurjchem-1125	305	11	,	,	PUNCT
eurjchem-1125	305	12	p.	p.	PROPN
eurjchem-1125	305	13	r.	r.	PROPN
eurjchem-1125	305	14	;	;	PUNCT
eurjchem-1125	305	15	xavier	xavier	PROPN
eurjchem-1125	305	16	,	,	PUNCT
eurjchem-1125	305	17	f.	f.	PROPN
eurjchem-1125	305	18	p.	p.	PROPN
eurjchem-1125	305	19	;	;	PUNCT
eurjchem-1125	305	20	vasu	vasu	PROPN
eurjchem-1125	305	21	,	,	PUNCT
eurjchem-1125	305	22	k.	k.	PROPN
eurjchem-1125	305	23	k.	k.	PROPN
eurjchem-1125	305	24	;	;	PUNCT
eurjchem-1125	305	25	padh	padh	PROPN
eurjchem-1125	305	26	,	,	PUNCT
eurjchem-1125	305	27	h.	h.	PROPN
eurjchem-1125	305	28	;	;	PUNCT
eurjchem-1125	305	29	sudarsanam	sudarsanam	NOUN
eurjchem-1125	305	30	,	,	PUNCT
eurjchem-1125	305	31	v.	v.	X
eurjchem-1125	305	32	bioorg	bioorg	VERB
eurjchem-1125	305	33	.	.	PUNCT
eurjchem-1125	306	1	med	med	PROPN
eurjchem-1125	306	2	.	.	PROPN
eurjchem-1125	306	3	chem	chem	PROPN
eurjchem-1125	306	4	.	.	PUNCT
eurjchem-1125	307	1	2005	2005	NUM
eurjchem-1125	307	2	,	,	PUNCT
eurjchem-1125	307	3	13	13	NUM
eurjchem-1125	307	4	,	,	PUNCT
eurjchem-1125	307	5	1275‐1283	1275‐1283	NUM
eurjchem-1125	307	6	.	.	PUNCT
eurjchem-1125	308	1	[	[	X
eurjchem-1125	308	2	4	4	NUM
eurjchem-1125	308	3	]	]	PUNCT
eurjchem-1125	308	4	.	.	PUNCT
eurjchem-1125	308	5	sabnis	sabnis	PROPN
eurjchem-1125	308	6	,	,	PUNCT
eurjchem-1125	308	7	r.	r.	PROPN
eurjchem-1125	308	8	w.	w.	PROPN
eurjchem-1125	308	9	;	;	PUNCT
eurjchem-1125	308	10	rangnekar	rangnekar	PROPN
eurjchem-1125	308	11	,	,	PUNCT
eurjchem-1125	308	12	d.	d.	PROPN
eurjchem-1125	308	13	w.	w.	PROPN
eurjchem-1125	308	14	;	;	PUNCT
eurjchem-1125	308	15	sonawane	sonawane	NOUN
eurjchem-1125	308	16	,	,	PUNCT
eurjchem-1125	308	17	n.	n.	PROPN
eurjchem-1125	308	18	d.	d.	PROPN
eurjchem-1125	308	19	j.	j.	PROPN
eurjchem-1125	308	20	heterocycl	heterocycl	PROPN
eurjchem-1125	308	21	.	.	PUNCT
eurjchem-1125	309	1	chem	chem	PROPN
eurjchem-1125	309	2	.	.	PUNCT
eurjchem-1125	310	1	1999	1999	NUM
eurjchem-1125	310	2	,	,	PUNCT
eurjchem-1125	310	3	36	36	NUM
eurjchem-1125	310	4	,	,	PUNCT
eurjchem-1125	310	5	333‐345	333‐345	NUM
eurjchem-1125	310	6	.	.	PUNCT
eurjchem-1125	311	1	[	[	X
eurjchem-1125	311	2	5	5	NUM
eurjchem-1125	311	3	]	]	PUNCT
eurjchem-1125	311	4	.	.	PUNCT
eurjchem-1125	312	1	ried	rie	VERB
eurjchem-1125	312	2	,	,	PUNCT
eurjchem-1125	312	3	w.	w.	PROPN
eurjchem-1125	312	4	;	;	PUNCT
eurjchem-1125	312	5	schleimer	schleimer	PROPN
eurjchem-1125	312	6	,	,	PUNCT
eurjchem-1125	312	7	b.	b.	PROPN
eurjchem-1125	312	8	angew	angew	PROPN
eurjchem-1125	312	9	.	.	PUNCT
eurjchem-1125	313	1	chem	chem	PROPN
eurjchem-1125	313	2	.	.	PUNCT
eurjchem-1125	314	1	1958	1958	NUM
eurjchem-1125	314	2	,	,	PUNCT
eurjchem-1125	314	3	70	70	NUM
eurjchem-1125	314	4	,	,	PUNCT
eurjchem-1125	314	5	164‐169	164‐169	NUM
eurjchem-1125	314	6	.	.	PUNCT
eurjchem-1125	315	1	[	[	X
eurjchem-1125	315	2	6	6	NUM
eurjchem-1125	315	3	]	]	PUNCT
eurjchem-1125	315	4	.	.	PUNCT
eurjchem-1125	316	1	stetinova	stetinova	PROPN
eurjchem-1125	316	2	,	,	PUNCT
eurjchem-1125	316	3	j.	j.	PROPN
eurjchem-1125	316	4	;	;	PUNCT
eurjchem-1125	316	5	kada	kada	PROPN
eurjchem-1125	316	6	,	,	PUNCT
eurjchem-1125	316	7	r.	r.	PROPN
eurjchem-1125	316	8	;	;	PUNCT
eurjchem-1125	316	9	lesko	lesko	PROPN
eurjchem-1125	316	10	,	,	PUNCT
eurjchem-1125	316	11	j.	j.	PROPN
eurjchem-1125	316	12	molecules	molecule	NOUN
eurjchem-1125	316	13	1996	1996	NUM
eurjchem-1125	316	14	,	,	PUNCT
eurjchem-1125	316	15	1	1	NUM
eurjchem-1125	316	16	,	,	PUNCT
eurjchem-1125	316	17	251‐254	251‐254	NOUN
eurjchem-1125	316	18	.	.	PUNCT
eurjchem-1125	317	1	[	[	X
eurjchem-1125	317	2	7	7	NUM
eurjchem-1125	317	3	]	]	PUNCT
eurjchem-1125	317	4	.	.	PUNCT
eurjchem-1125	318	1	gorobets	gorobet	NOUN
eurjchem-1125	318	2	,	,	PUNCT
eurjchem-1125	318	3	n.	n.	PROPN
eurjchem-1125	318	4	y	y	PROPN
eurjchem-1125	318	5	;	;	PUNCT
eurjchem-1125	318	6	yousefi	yousefi	PROPN
eurjchem-1125	318	7	,	,	PUNCT
eurjchem-1125	318	8	b.	b.	PROPN
eurjchem-1125	318	9	h.	h.	PROPN
eurjchem-1125	318	10	;	;	PUNCT
eurjchem-1125	318	11	belaj	belaj	NOUN
eurjchem-1125	318	12	,	,	PUNCT
eurjchem-1125	318	13	f.	f.	PROPN
eurjchem-1125	318	14	;	;	PUNCT
eurjchem-1125	318	15	kappe	kappe	PROPN
eurjchem-1125	318	16	,	,	PUNCT
eurjchem-1125	318	17	c.	c.	PROPN
eurjchem-1125	318	18	o.	o.	PROPN
eurjchem-1125	318	19	tetrahedron	tetrahedron	PROPN
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eurjchem-1125	318	21	,	,	PUNCT
eurjchem-1125	318	22	60	60	NUM
eurjchem-1125	318	23	,	,	PUNCT
eurjchem-1125	318	24	8633‐8644	8633‐8644	NUM
eurjchem-1125	318	25	.	.	PUNCT
eurjchem-1125	319	1	[	[	X
eurjchem-1125	319	2	8	8	NUM
eurjchem-1125	319	3	]	]	PUNCT
eurjchem-1125	319	4	.	.	PUNCT
eurjchem-1125	319	5	gouda	gouda	NOUN
eurjchem-1125	319	6	,	,	PUNCT
eurjchem-1125	319	7	m.	m.	NOUN
eurjchem-1125	319	8	a.	a.	NOUN
eurjchem-1125	319	9	;	;	PUNCT
eurjchem-1125	319	10	abu‐hashem	abu‐hashem	PROPN
eurjchem-1125	319	11	,	,	PUNCT
eurjchem-1125	319	12	a.	a.	NOUN
eurjchem-1125	319	13	a.	a.	NOUN
eurjchem-1125	319	14	arch	arch	NOUN
eurjchem-1125	319	15	.	.	PUNCT
eurjchem-1125	320	1	pharm	pharm	NOUN
eurjchem-1125	320	2	.	.	PUNCT
eurjchem-1125	321	1	2011	2011	NUM
eurjchem-1125	321	2	,	,	PUNCT
eurjchem-1125	321	3	11	11	NUM
eurjchem-1125	321	4	,	,	PUNCT
eurjchem-1125	321	5	170‐177	170‐177	NUM
eurjchem-1125	321	6	.	.	PUNCT
eurjchem-1125	322	1	[	[	X
eurjchem-1125	322	2	9	9	NUM
eurjchem-1125	322	3	]	]	PUNCT
eurjchem-1125	322	4	.	.	PUNCT
eurjchem-1125	322	5	gutteridge	gutteridge	PROPN
eurjchem-1125	322	6	,	,	PUNCT
eurjchem-1125	322	7	j.	j.	PROPN
eurjchem-1125	322	8	m.	m.	PROPN
eurjchem-1125	322	9	c.	c.	PROPN
eurjchem-1125	322	10	free	free	PROPN
eurjchem-1125	322	11	radic	radic	NOUN
eurjchem-1125	322	12	.	.	PUNCT
eurjchem-1125	323	1	res	re	NOUN
eurjchem-1125	323	2	.	.	PUNCT
eurjchem-1125	324	1	commun	commun	PROPN
eurjchem-1125	324	2	.	.	PUNCT
eurjchem-1125	325	1	1993	1993	NUM
eurjchem-1125	325	2	,	,	PUNCT
eurjchem-1125	325	3	19	19	NUM
eurjchem-1125	325	4	,	,	PUNCT
eurjchem-1125	325	5	141‐158	141‐158	NUM
eurjchem-1125	325	6	.	.	PUNCT
eurjchem-1125	326	1	[	[	X
eurjchem-1125	326	2	10	10	NUM
eurjchem-1125	326	3	]	]	PUNCT
eurjchem-1125	326	4	.	.	PUNCT
eurjchem-1125	327	1	kehrer	kehrer	PROPN
eurjchem-1125	327	2	,	,	PUNCT
eurjchem-1125	327	3	j.	j.	PROPN
eurjchem-1125	327	4	p.	p.	PROPN
eurjchem-1125	327	5	crit	crit	PROPN
eurjchem-1125	327	6	.	.	PUNCT
eurjchem-1125	328	1	rev	rev	PROPN
eurjchem-1125	328	2	.	.	PROPN
eurjchem-1125	329	1	toxicol	toxicol	PROPN
eurjchem-1125	329	2	.	.	PUNCT
eurjchem-1125	329	3	1993	1993	NUM
eurjchem-1125	329	4	,	,	PUNCT
eurjchem-1125	329	5	23	23	NUM
eurjchem-1125	329	6	,	,	PUNCT
eurjchem-1125	329	7	21‐48	21‐48	NUM
eurjchem-1125	329	8	.	.	PUNCT
eurjchem-1125	330	1	[	[	X
eurjchem-1125	330	2	11	11	NUM
eurjchem-1125	330	3	]	]	PUNCT
eurjchem-1125	330	4	.	.	PUNCT
eurjchem-1125	330	5	becker	becker	PROPN
eurjchem-1125	330	6	,	,	PUNCT
eurjchem-1125	330	7	l.	l.	PROPN
eurjchem-1125	330	8	b.	b.	PROPN
eurjchem-1125	330	9	cardiovasc	cardiovasc	PROPN
eurjchem-1125	330	10	res	res	PROPN
eurjchem-1125	330	11	.	.	PUNCT
eurjchem-1125	330	12	2004	2004	NUM
eurjchem-1125	330	13	,	,	PUNCT
eurjchem-1125	330	14	61	61	NUM
eurjchem-1125	330	15	,	,	PUNCT
eurjchem-1125	330	16	461‐470	461‐470	NOUN
eurjchem-1125	330	17	.	.	PUNCT
eurjchem-1125	331	1	[	[	X
eurjchem-1125	331	2	12	12	NUM
eurjchem-1125	331	3	]	]	PUNCT
eurjchem-1125	331	4	.	.	PUNCT
eurjchem-1125	332	1	hayes	hayes	PROPN
eurjchem-1125	332	2	,	,	PUNCT
eurjchem-1125	332	3	j.	j.	PROPN
eurjchem-1125	332	4	d.	d.	PROPN
eurjchem-1125	332	5	;	;	PUNCT
eurjchem-1125	332	6	mclellan	mclellan	PROPN
eurjchem-1125	332	7	,	,	PUNCT
eurjchem-1125	332	8	l.	l.	PROPN
eurjchem-1125	332	9	i.	i.	PROPN
eurjchem-1125	332	10	free	free	PROPN
eurjchem-1125	332	11	radic	radic	PROPN
eurjchem-1125	332	12	.	.	PUNCT
eurjchem-1125	333	1	res	re	NOUN
eurjchem-1125	333	2	.	.	PROPN
eurjchem-1125	333	3	1999	1999	NUM
eurjchem-1125	333	4	,	,	PUNCT
eurjchem-1125	333	5	31	31	NUM
eurjchem-1125	333	6	,	,	PUNCT
eurjchem-1125	333	7	273‐300	273‐300	NUM
eurjchem-1125	333	8	.	.	PUNCT
eurjchem-1125	334	1	[	[	X
eurjchem-1125	334	2	13	13	NUM
eurjchem-1125	334	3	]	]	PUNCT
eurjchem-1125	334	4	.	.	PUNCT
eurjchem-1125	335	1	masella	masella	PROPN
eurjchem-1125	335	2	,	,	PUNCT
eurjchem-1125	335	3	r.	r.	PROPN
eurjchem-1125	335	4	;	;	PUNCT
eurjchem-1125	335	5	di	di	X
eurjchem-1125	335	6	benedetto	benedetto	PROPN
eurjchem-1125	335	7	,	,	PUNCT
eurjchem-1125	335	8	r.	r.	PROPN
eurjchem-1125	335	9	;	;	PUNCT
eurjchem-1125	335	10	vari	vari	PROPN
eurjchem-1125	335	11	,	,	PUNCT
eurjchem-1125	335	12	r.	r.	PROPN
eurjchem-1125	335	13	;	;	PUNCT
eurjchem-1125	335	14	filesi	filesi	PROPN
eurjchem-1125	335	15	,	,	PUNCT
eurjchem-1125	335	16	c.	c.	PROPN
eurjchem-1125	335	17	;	;	PUNCT
eurjchem-1125	335	18	giovannini	giovannini	PROPN
eurjchem-1125	335	19	,	,	PUNCT
eurjchem-1125	335	20	c.	c.	PROPN
eurjchem-1125	335	21	j.	j.	PROPN
eurjchem-1125	335	22	nutr	nutr	PROPN
eurjchem-1125	335	23	.	.	PROPN
eurjchem-1125	335	24	biochem	biochem	PROPN
eurjchem-1125	335	25	.	.	PUNCT
eurjchem-1125	336	1	2005	2005	NUM
eurjchem-1125	336	2	,	,	PUNCT
eurjchem-1125	336	3	16	16	NUM
eurjchem-1125	336	4	,	,	PUNCT
eurjchem-1125	336	5	577‐586	577‐586	NUM
eurjchem-1125	336	6	.	.	PUNCT
eurjchem-1125	337	1	[	[	X
eurjchem-1125	337	2	14	14	NUM
eurjchem-1125	337	3	]	]	PUNCT
eurjchem-1125	337	4	.	.	PUNCT
eurjchem-1125	338	1	hartmann	hartmann	PROPN
eurjchem-1125	338	2	,	,	PUNCT
eurjchem-1125	338	3	r.	r.	PROPN
eurjchem-1125	338	4	e.	e.	PROPN
eurjchem-1125	338	5	;	;	PUNCT
eurjchem-1125	338	6	shah	shah	PROPN
eurjchem-1125	338	7	,	,	PUNCT
eurjchem-1125	338	8	a.	a.	NOUN
eurjchem-1125	338	9	;	;	PUNCT
eurjchem-1125	338	10	fagan	fagan	PROPN
eurjchem-1125	338	11	,	,	PUNCT
eurjchem-1125	338	12	a.	a.	NOUN
eurjchem-1125	338	13	m.	m.	NOUN
eurjchem-1125	338	14	;	;	PUNCT
eurjchem-1125	338	15	schwetye	schwetye	PROPN
eurjchem-1125	338	16	,	,	PUNCT
eurjchem-1125	338	17	k.	k.	PROPN
eurjchem-1125	338	18	e.	e.	PROPN
eurjchem-1125	338	19	;	;	PUNCT
eurjchem-1125	338	20	parsadanian	parsadanian	ADJ
eurjchem-1125	338	21	,	,	PUNCT
eurjchem-1125	338	22	m.	m.	NOUN
eurjchem-1125	338	23	;	;	PUNCT
eurjchem-1125	338	24	schulman	schulman	PROPN
eurjchem-1125	338	25	,	,	PUNCT
eurjchem-1125	338	26	r.	r.	PROPN
eurjchem-1125	338	27	n.	n.	PROPN
eurjchem-1125	338	28	;	;	PUNCT
eurjchem-1125	338	29	finn	finn	PROPN
eurjchem-1125	338	30	,	,	PUNCT
eurjchem-1125	338	31	m.	m.	PROPN
eurjchem-1125	338	32	b.	b.	PROPN
eurjchem-1125	338	33	;	;	PUNCT
eurjchem-1125	338	34	holtzman	holtzman	PROPN
eurjchem-1125	338	35	,	,	PUNCT
eurjchem-1125	338	36	d.	d.	PROPN
eurjchem-1125	338	37	m.	m.	PROPN
eurjchem-1125	338	38	neurobiol	neurobiol	PROPN
eurjchem-1125	338	39	dis	dis	PROPN
eurjchem-1125	338	40	.	.	PUNCT
eurjchem-1125	339	1	2006	2006	NUM
eurjchem-1125	339	2	,	,	PUNCT
eurjchem-1125	339	3	24	24	NUM
eurjchem-1125	339	4	,	,	PUNCT
eurjchem-1125	339	5	506‐515	506‐515	NUM
eurjchem-1125	339	6	.	.	PUNCT
eurjchem-1125	340	1	[	[	X
eurjchem-1125	340	2	15	15	NUM
eurjchem-1125	340	3	]	]	PUNCT
eurjchem-1125	340	4	.	.	PUNCT
eurjchem-1125	341	1	hollman	hollman	NOUN
eurjchem-1125	341	2	,	,	PUNCT
eurjchem-1125	341	3	p.	p.	PROPN
eurjchem-1125	341	4	c.	c.	PROPN
eurjchem-1125	341	5	;	;	PUNCT
eurjchem-1125	341	6	van	van	PROPN
eurjchem-1125	341	7	trijp	trijp	PROPN
eurjchem-1125	341	8	,	,	PUNCT
eurjchem-1125	341	9	j.	j.	PROPN
eurjchem-1125	341	10	m.	m.	PROPN
eurjchem-1125	341	11	;	;	PUNCT
eurjchem-1125	341	12	buysman	buysman	NOUN
eurjchem-1125	341	13	,	,	PUNCT
eurjchem-1125	341	14	m.	m.	NOUN
eurjchem-1125	341	15	n.	n.	NOUN
eurjchem-1125	341	16	;	;	PUNCT
eurjchem-1125	341	17	van	van	PROPN
eurjchem-1125	341	18	der	der	NOUN
eurjchem-1125	341	19	gaag	gaag	VERB
eurjchem-1125	341	20	,	,	PUNCT
eurjchem-1125	341	21	m.	m.	NOUN
eurjchem-1125	341	22	s.	s.	PROPN
eurjchem-1125	341	23	;	;	PUNCT
eurjchem-1125	341	24	mengelers	mengeler	NOUN
eurjchem-1125	341	25	,	,	PUNCT
eurjchem-1125	341	26	m.	m.	NOUN
eurjchem-1125	341	27	j.	j.	PROPN
eurjchem-1125	341	28	;	;	PUNCT
eurjchem-1125	341	29	de	de	PROPN
eurjchem-1125	341	30	vries	vries	PROPN
eurjchem-1125	341	31	,	,	PUNCT
eurjchem-1125	341	32	j.	j.	PROPN
eurjchem-1125	341	33	h.	h.	PROPN
eurjchem-1125	341	34	;	;	PUNCT
eurjchem-1125	341	35	katan	katan	PROPN
eurjchem-1125	341	36	,	,	PUNCT
eurjchem-1125	341	37	m.	m.	PROPN
eurjchem-1125	341	38	b.	b.	PROPN
eurjchem-1125	341	39	febs	febs	PROPN
eurjchem-1125	341	40	lett	lett	PROPN
eurjchem-1125	341	41	.	.	PUNCT
eurjchem-1125	342	1	1997	1997	NUM
eurjchem-1125	342	2	,	,	PUNCT
eurjchem-1125	342	3	418	418	NUM
eurjchem-1125	342	4	,	,	PUNCT
eurjchem-1125	342	5	152‐	152‐	NUM
eurjchem-1125	342	6	156	156	NUM
eurjchem-1125	342	7	.	.	PUNCT
eurjchem-1125	343	1	[	[	X
eurjchem-1125	343	2	16	16	NUM
eurjchem-1125	343	3	]	]	PUNCT
eurjchem-1125	343	4	.	.	PUNCT
eurjchem-1125	344	1	abu‐hashem	abu‐hashem	PROPN
eurjchem-1125	344	2	,	,	PUNCT
eurjchem-1125	344	3	a.	a.	NOUN
eurjchem-1125	344	4	a.	a.	NOUN
eurjchem-1125	344	5	;	;	PUNCT
eurjchem-1125	344	6	el‐shehry	el‐shehry	NOUN
eurjchem-1125	344	7	,	,	PUNCT
eurjchem-1125	344	8	m.	m.	NOUN
eurjchem-1125	344	9	f.	f.	PROPN
eurjchem-1125	344	10	;	;	PUNCT
eurjchem-1125	344	11	badria	badria	PROPN
eurjchem-1125	344	12	,	,	PUNCT
eurjchem-1125	344	13	f.	f.	PROPN
eurjchem-1125	344	14	a.	a.	PROPN
eurjchem-1125	344	15	acta	acta	PROPN
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eurjchem-1125	344	17	.	.	PUNCT
eurjchem-1125	345	1	2010	2010	NUM
eurjchem-1125	345	2	,	,	PUNCT
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eurjchem-1125	345	4	,	,	PUNCT
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eurjchem-1125	345	6	.	.	PUNCT
eurjchem-1125	346	1	[	[	X
eurjchem-1125	346	2	17	17	NUM
eurjchem-1125	346	3	]	]	PUNCT
eurjchem-1125	346	4	.	.	PUNCT
eurjchem-1125	347	1	gewald	gewald	NOUN
eurjchem-1125	347	2	,	,	PUNCT
eurjchem-1125	347	3	k.	k.	PROPN
eurjchem-1125	347	4	chem	chem	PROPN
eurjchem-1125	347	5	.	.	PUNCT
eurjchem-1125	348	1	ber	ber	PROPN
eurjchem-1125	348	2	.	.	PUNCT
eurjchem-1125	349	1	1965	1965	NUM
eurjchem-1125	349	2	,	,	PUNCT
eurjchem-1125	349	3	98	98	NUM
eurjchem-1125	349	4	,	,	PUNCT
eurjchem-1125	349	5	3571‐3577	3571‐3577	NUM
eurjchem-1125	349	6	.	.	PUNCT
eurjchem-1125	350	1	[	[	X
eurjchem-1125	350	2	18	18	NUM
eurjchem-1125	350	3	]	]	PUNCT
eurjchem-1125	350	4	.	.	PUNCT
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eurjchem-1125	351	2	,	,	PUNCT
eurjchem-1125	351	3	n.	n.	PROPN
eurjchem-1125	351	4	y.	y.	PROPN
eurjchem-1125	351	5	;	;	PUNCT
eurjchem-1125	351	6	yousefi	yousefi	PROPN
eurjchem-1125	351	7	,	,	PUNCT
eurjchem-1125	351	8	b.	b.	PROPN
eurjchem-1125	351	9	h.	h.	PROPN
eurjchem-1125	351	10	;	;	PUNCT
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eurjchem-1125	351	12	,	,	PUNCT
eurjchem-1125	351	13	f.	f.	PROPN
eurjchem-1125	351	14	;	;	PUNCT
eurjchem-1125	351	15	kappe	kappe	PROPN
eurjchem-1125	351	16	,	,	PUNCT
eurjchem-1125	351	17	c.	c.	PROPN
eurjchem-1125	351	18	o.	o.	PROPN
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eurjchem-1125	351	21	,	,	PUNCT
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eurjchem-1125	351	23	,	,	PUNCT
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eurjchem-1125	351	25	.	.	PUNCT
eurjchem-1125	352	1	[	[	X
eurjchem-1125	352	2	19	19	NUM
eurjchem-1125	352	3	]	]	PUNCT
eurjchem-1125	352	4	.	.	PUNCT
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eurjchem-1125	353	2	,	,	PUNCT
eurjchem-1125	353	3	m.	m.	NOUN
eurjchem-1125	353	4	;	;	PUNCT
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eurjchem-1125	353	6	,	,	PUNCT
eurjchem-1125	353	7	n.	n.	PROPN
eurjchem-1125	353	8	a.	a.	PROPN
eurjchem-1125	353	9	;	;	PUNCT
eurjchem-1125	353	10	yagi	yagi	PROPN
eurjchem-1125	353	11	,	,	PUNCT
eurjchem-1125	353	12	k.	k.	PROPN
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eurjchem-1125	353	14	.	.	PUNCT
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eurjchem-1125	354	2	.	.	PUNCT
eurjchem-1125	355	1	res	re	NOUN
eurjchem-1125	355	2	.	.	PROPN
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eurjchem-1125	355	4	.	.	PUNCT
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eurjchem-1125	356	2	,	,	PUNCT
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eurjchem-1125	356	4	,	,	PUNCT
eurjchem-1125	356	5	849‐853	849‐853	NOUN
eurjchem-1125	356	6	.	.	PUNCT
eurjchem-1125	357	1	[	[	X
eurjchem-1125	357	2	20	20	NUM
eurjchem-1125	357	3	]	]	PUNCT
eurjchem-1125	357	4	.	.	PUNCT
eurjchem-1125	358	1	aeschbach	aeschbach	PROPN
eurjchem-1125	358	2	,	,	PUNCT
eurjchem-1125	358	3	r.	r.	PROPN
eurjchem-1125	358	4	;	;	PUNCT
eurjchem-1125	358	5	löliger	löliger	PROPN
eurjchem-1125	358	6	,	,	PUNCT
eurjchem-1125	358	7	j.	j.	PROPN
eurjchem-1125	358	8	;	;	PUNCT
eurjchem-1125	358	9	scott	scott	PROPN
eurjchem-1125	358	10	,	,	PUNCT
eurjchem-1125	358	11	b.	b.	PROPN
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eurjchem-1125	358	13	;	;	PUNCT
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eurjchem-1125	358	15	,	,	PUNCT
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eurjchem-1125	358	17	;	;	PUNCT
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eurjchem-1125	358	19	,	,	PUNCT
eurjchem-1125	358	20	j.	j.	PROPN
eurjchem-1125	358	21	;	;	PUNCT
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eurjchem-1125	358	23	,	,	PUNCT
eurjchem-1125	358	24	b.	b.	PROPN
eurjchem-1125	358	25	;	;	PUNCT
eurjchem-1125	358	26	o.	o.	PROPN
eurjchem-1125	358	27	;	;	PUNCT
eurjchem-1125	358	28	aruoma	aruoma	PROPN
eurjchem-1125	358	29	,	,	PUNCT
eurjchem-1125	358	30	i.	i.	PROPN
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eurjchem-1125	358	33	.	.	PUNCT
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eurjchem-1125	359	2	.	.	PROPN
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eurjchem-1125	359	4	,	,	PUNCT
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eurjchem-1125	359	6	,	,	PUNCT
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eurjchem-1125	359	8	[	[	X
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eurjchem-1125	359	10	]	]	PUNCT
eurjchem-1125	359	11	.	.	PUNCT
eurjchem-1125	360	1	farghaly	farghaly	PROPN
eurjchem-1125	360	2	,	,	PUNCT
eurjchem-1125	360	3	t.	t.	PROPN
eurjchem-1125	360	4	a.	a.	PROPN
eurjchem-1125	360	5	;	;	PUNCT
eurjchem-1125	360	6	abdallah	abdallah	PROPN
eurjchem-1125	360	7	,	,	PUNCT
eurjchem-1125	360	8	zeinab	zeinab	PROPN
eurjchem-1125	360	9	a.	a.	NOUN
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eurjchem-1125	361	1	[	[	X
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eurjchem-1125	361	3	]	]	PUNCT
eurjchem-1125	361	4	.	.	PUNCT
eurjchem-1125	362	1	darwish	darwish	PROPN
eurjchem-1125	362	2	,	,	PUNCT
eurjchem-1125	362	3	elham	elham	PROPN
eurjchem-1125	362	4	s.	s.	PROPN
eurjchem-1125	362	5	;	;	PUNCT
eurjchem-1125	362	6	abdel	abdel	PROPN
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eurjchem-1125	362	8	,	,	PUNCT
eurjchem-1125	362	9	azza	azza	PROPN
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eurjchem-1125	362	11	;	;	PUNCT
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eurjchem-1125	362	14	a.	a.	PROPN
eurjchem-1125	362	15	;	;	PUNCT
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eurjchem-1125	362	17	,	,	PUNCT
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eurjchem-1125	362	21	.	.	PUNCT
eurjchem-1125	363	1	j.	j.	PROPN
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eurjchem-1125	363	3	.	.	PUNCT
eurjchem-1125	364	1	sci	sci	PROPN
eurjchem-1125	364	2	.	.	PROPN
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eurjchem-1125	364	4	,	,	PUNCT
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eurjchem-1125	364	8	.	.	PUNCT
eurjchem-1125	365	1	[	[	X
eurjchem-1125	365	2	23	23	NUM
eurjchem-1125	365	3	]	]	PUNCT
eurjchem-1125	365	4	.	.	PUNCT
eurjchem-1125	366	1	ammar	ammar	PROPN
eurjchem-1125	366	2	,	,	PUNCT
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eurjchem-1125	366	4	a.	a.	PROPN
eurjchem-1125	366	5	;	;	PUNCT
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eurjchem-1125	366	7	,	,	PUNCT
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eurjchem-1125	366	10	;	;	PUNCT
eurjchem-1125	366	11	salem	salem	NOUN
eurjchem-1125	366	12	,	,	PUNCT
eurjchem-1125	366	13	m.	m.	NOUN
eurjchem-1125	366	14	a.	a.	PROPN
eurjchem-1125	366	15	;	;	PUNCT
eurjchem-1125	366	16	al‐sehemi	al‐sehemi	PROPN
eurjchem-1125	366	17	,	,	PUNCT
eurjchem-1125	366	18	abd	abd	PROPN
eurjchem-1125	366	19	allah	allah	PROPN
eurjchem-1125	366	20	g.	g.	PROPN
eurjchem-1125	366	21	;	;	PUNCT
eurjchem-1125	366	22	el‐	el‐	PROPN
eurjchem-1125	366	23	gaby	gaby	NOUN
eurjchem-1125	366	24	,	,	PUNCT
eurjchem-1125	366	25	m.	m.	PROPN
eurjchem-1125	366	26	s.	s.	PROPN
eurjchem-1125	366	27	a.	a.	PROPN
eurjchem-1125	366	28	j.	j.	PROPN
eurjchem-1125	366	29	chin	chin	PROPN
eurjchem-1125	366	30	.	.	PROPN
eurjchem-1125	366	31	chem	chem	PROPN
eurjchem-1125	366	32	.	.	PUNCT
eurjchem-1125	366	33	soc‐taip	soc‐taip	PROPN
eurjchem-1125	366	34	2009	2009	NUM
eurjchem-1125	366	35	,	,	PUNCT
eurjchem-1125	366	36	56	56	NUM
eurjchem-1125	366	37	,	,	PUNCT
eurjchem-1125	366	38	1064‐	1064‐	NUM
eurjchem-1125	366	39	1071	1071	NUM
eurjchem-1125	366	40	.	.	PUNCT