id sid tid token lemma pos eurjchem-116 1 1 microsoft microsoft PROPN eurjchem-116 1 2 word word NOUN eurjchem-116 1 3 european_journal_of_chemistry_1_4_2010_262_265_116 european_journal_of_chemistry_1_4_2010_262_265_116 ADP eurjchem-116 1 4 european european ADJ eurjchem-116 1 5     SPACE eurjchem-116 1 6 journal journal NOUN eurjchem-116 1 7     SPACE eurjchem-116 1 8 of of ADP eurjchem-116 1 9     SPACE eurjchem-116 1 10 chemistry chemistry NOUN eurjchem-116 1 11     SPACE eurjchem-116 1 12 1 1 NUM eurjchem-116 1 13     SPACE eurjchem-116 1 14 ( ( PUNCT eurjchem-116 1 15 4 4 NUM eurjchem-116 1 16 ) ) PUNCT eurjchem-116 1 17     SPACE eurjchem-116 1 18 ( ( PUNCT eurjchem-116 1 19 2010 2010 NUM eurjchem-116 1 20 ) ) PUNCT eurjchem-116 1 21     SPACE eurjchem-116 1 22 262‐265 262‐265 NOUN eurjchem-116 1 23         SPACE eurjchem-116 1 24 european european ADJ eurjchem-116 1 25     SPACE eurjchem-116 1 26 journal journal NOUN eurjchem-116 1 27     SPACE eurjchem-116 1 28 of of ADP eurjchem-116 1 29     SPACE eurjchem-116 1 30 chemistry chemistry NOUN eurjchem-116 1 31     SPACE eurjchem-116 1 32 issn issn VERB eurjchem-116 1 33     SPACE eurjchem-116 1 34 2153‐2249 2153‐2249 NUM eurjchem-116 1 35     SPACE eurjchem-116 1 36 ( ( PUNCT eurjchem-116 1 37 print print NOUN eurjchem-116 1 38 ) ) PUNCT eurjchem-116 1 39     SPACE eurjchem-116 1 40 / / SYM eurjchem-116 1 41     SPACE eurjchem-116 1 42 issn issn VERB eurjchem-116 1 43     SPACE eurjchem-116 1 44 2153‐2257 2153‐2257 NUM eurjchem-116 1 45     SPACE eurjchem-116 1 46 ( ( PUNCT eurjchem-116 1 47 online online ADJ eurjchem-116 1 48 ) ) PUNCT eurjchem-116 1 49     SPACE eurjchem-116 1 50   NOUN eurjchem-116 1 51     SPACE eurjchem-116 1 52 2010 2010 NUM eurjchem-116 1 53     SPACE eurjchem-116 1 54 eurjchem eurjchem NOUN eurjchem-116 1 55     SPACE eurjchem-116 1 56 doi:10.5155 doi:10.5155 PROPN eurjchem-116 1 57 / / SYM eurjchem-116 1 58 eurjchem.1.4.262‐265.116 eurjchem.1.4.262‐265.116 ADJ eurjchem-116 1 59                 SPACE eurjchem-116 1 60 european european ADJ eurjchem-116 1 61     SPACE eurjchem-116 1 62 journal journal NOUN eurjchem-116 1 63     SPACE eurjchem-116 1 64 of of ADP eurjchem-116 1 65     SPACE eurjchem-116 1 66 chemistry chemistry NOUN eurjchem-116 1 67     SPACE eurjchem-116 1 68 journal journal NOUN eurjchem-116 1 69     SPACE eurjchem-116 1 70 homepage homepage NOUN eurjchem-116 1 71 : : PUNCT eurjchem-116 1 72     SPACE eurjchem-116 1 73 www.eurjchem.com www.eurjchem.com NOUN eurjchem-116 1 74                     SPACE eurjchem-116 1 75 determination determination NOUN eurjchem-116 1 76     SPACE eurjchem-116 1 77 of of ADP eurjchem-116 1 78     SPACE eurjchem-116 1 79 voglibose voglibose NOUN eurjchem-116 1 80     SPACE eurjchem-116 1 81 in in ADP eurjchem-116 1 82     SPACE eurjchem-116 1 83 pharmaceutical pharmaceutical NOUN eurjchem-116 1 84     SPACE eurjchem-116 1 85 formulations formulation NOUN eurjchem-116 1 86     SPACE eurjchem-116 1 87 by by ADP eurjchem-116 1 88     SPACE eurjchem-116 1 89 high high ADJ eurjchem-116 1 90     SPACE eurjchem-116 1 91 performance performance NOUN eurjchem-116 1 92     SPACE eurjchem-116 1 93 liquid liquid NOUN eurjchem-116 1 94     SPACE eurjchem-116 1 95 chromatography chromatography NOUN eurjchem-116 1 96     SPACE eurjchem-116 1 97 using use VERB eurjchem-116 1 98     SPACE eurjchem-116 1 99 refractive refractive ADJ eurjchem-116 1 100     SPACE eurjchem-116 1 101 index index NOUN eurjchem-116 1 102     SPACE eurjchem-116 1 103 detection detection NOUN eurjchem-116 1 104     SPACE eurjchem-116 1 105 karunanidhi karunanidhi PROPN eurjchem-116 1 106     SPACE eurjchem-116 1 107 lakshmi lakshmi PROPN eurjchem-116 1 108     SPACE eurjchem-116 1 109 and and CCONJ eurjchem-116 1 110     SPACE eurjchem-116 1 111 tirumala tirumala NOUN eurjchem-116 1 112     SPACE eurjchem-116 1 113 rajesh rajesh PROPN eurjchem-116 1 114 * * PUNCT eurjchem-116 1 115     SPACE eurjchem-116 1 116 department department NOUN eurjchem-116 1 117     SPACE eurjchem-116 1 118 of of ADP eurjchem-116 1 119     SPACE eurjchem-116 1 120 pharmaceutical pharmaceutical NOUN eurjchem-116 1 121     SPACE eurjchem-116 1 122 analysis analysis NOUN eurjchem-116 1 123 , , PUNCT eurjchem-116 1 124     SPACE eurjchem-116 1 125 college college NOUN eurjchem-116 1 126     SPACE eurjchem-116 1 127 of of ADP eurjchem-116 1 128     SPACE eurjchem-116 1 129 pharmacy pharmacy NOUN eurjchem-116 1 130 , , PUNCT eurjchem-116 1 131     SPACE eurjchem-116 1 132 sri sri NOUN eurjchem-116 1 133     SPACE eurjchem-116 1 134 ramasamy ramasamy NOUN eurjchem-116 1 135     SPACE eurjchem-116 1 136 memorial memorial ADJ eurjchem-116 1 137     SPACE eurjchem-116 1 138 university university NOUN eurjchem-116 1 139 , , PUNCT eurjchem-116 1 140     SPACE eurjchem-116 1 141 kattankulathur kattankulathur PROPN eurjchem-116 1 142 , , PUNCT eurjchem-116 1 143     SPACE eurjchem-116 1 144 in­603203 in­603203 PROPN eurjchem-116 1 145 , , PUNCT eurjchem-116 1 146     SPACE eurjchem-116 1 147 tamil tamil NOUN eurjchem-116 1 148     SPACE eurjchem-116 1 149 nadu nadu ADJ eurjchem-116 1 150 , , PUNCT eurjchem-116 1 151     SPACE eurjchem-116 1 152 india india PROPN eurjchem-116 1 153     SPACE eurjchem-116 1 154 * * PROPN eurjchem-116 1 155 corresponding correspond VERB eurjchem-116 1 156     SPACE eurjchem-116 1 157 author author NOUN eurjchem-116 1 158     SPACE eurjchem-116 1 159 at at ADP eurjchem-116 1 160 : : PUNCT eurjchem-116 1 161     SPACE eurjchem-116 1 162 department department NOUN eurjchem-116 1 163     SPACE eurjchem-116 1 164 of of ADP eurjchem-116 1 165     SPACE eurjchem-116 1 166 pharmaceutical pharmaceutical NOUN eurjchem-116 1 167     SPACE eurjchem-116 1 168 analysis analysis NOUN eurjchem-116 1 169 , , PUNCT eurjchem-116 1 170     SPACE eurjchem-116 1 171 college college NOUN eurjchem-116 1 172     SPACE eurjchem-116 1 173 of of ADP eurjchem-116 1 174     SPACE eurjchem-116 1 175 pharmacy pharmacy NOUN eurjchem-116 1 176 , , PUNCT eurjchem-116 1 177     SPACE eurjchem-116 1 178 sri sri NOUN eurjchem-116 1 179     SPACE eurjchem-116 1 180 ramasamy ramasamy NOUN eurjchem-116 1 181     SPACE eurjchem-116 1 182 memorial memorial ADJ eurjchem-116 1 183     SPACE eurjchem-116 1 184 university university NOUN eurjchem-116 1 185 , , PUNCT eurjchem-116 1 186     SPACE eurjchem-116 1 187 kattankulathur kattankulathur PROPN eurjchem-116 1 188 , , PUNCT eurjchem-116 1 189     SPACE eurjchem-116 1 190 in­603203 in­603203 PROPN eurjchem-116 1 191 , , PUNCT eurjchem-116 1 192       SPACE eurjchem-116 1 193 tamil tamil NOUN eurjchem-116 1 194     SPACE eurjchem-116 1 195 nadu nadu ADJ eurjchem-116 1 196 , , PUNCT eurjchem-116 1 197     SPACE eurjchem-116 1 198 india india PROPN eurjchem-116 1 199 . . PUNCT eurjchem-116 1 200     SPACE eurjchem-116 1 201 tel tel PROPN eurjchem-116 1 202 . . PUNCT eurjchem-116 1 203 : : PUNCT eurjchem-116 1 204     SPACE eurjchem-116 1 205 +91.442.7453160 +91.442.7453160 NUM eurjchem-116 1 206 ; ; PUNCT eurjchem-116 1 207     SPACE eurjchem-116 1 208 fax fax NOUN eurjchem-116 1 209 : : PUNCT eurjchem-116 1 210     SPACE eurjchem-116 1 211 +91.442.7455717 +91.442.7455717 PROPN eurjchem-116 1 212 . . PUNCT eurjchem-116 1 213     SPACE eurjchem-116 1 214 e­mail e­mail NOUN eurjchem-116 1 215     SPACE eurjchem-116 1 216 address address NOUN eurjchem-116 1 217 : : PUNCT eurjchem-116 1 218     SPACE eurjchem-116 1 219 rajeshtirumala@hotmail.com rajeshtirumala@hotmail.com X eurjchem-116 1 220       SPACE eurjchem-116 1 221 ( ( PUNCT eurjchem-116 1 222 t. t. NOUN eurjchem-116 1 223     SPACE eurjchem-116 1 224 rajesh rajesh PROPN eurjchem-116 1 225 ) ) PUNCT eurjchem-116 1 226 . . PUNCT eurjchem-116 1 227                                 SPACE eurjchem-116 2 1 article article NOUN eurjchem-116 2 2     SPACE eurjchem-116 2 3 information information NOUN eurjchem-116 2 4         SPACE eurjchem-116 2 5 abstract abstract ADJ eurjchem-116 2 6 received receive VERB eurjchem-116 2 7 : : PUNCT eurjchem-116 2 8     SPACE eurjchem-116 2 9 20 20 NUM eurjchem-116 2 10     SPACE eurjchem-116 2 11 may may AUX eurjchem-116 2 12     SPACE eurjchem-116 2 13 2010 2010 NUM eurjchem-116 2 14     SPACE eurjchem-116 2 15 received receive VERB eurjchem-116 2 16     SPACE eurjchem-116 2 17 in in ADP eurjchem-116 2 18     SPACE eurjchem-116 2 19 revised revise VERB eurjchem-116 2 20     SPACE eurjchem-116 2 21 form form NOUN eurjchem-116 2 22 : : PUNCT eurjchem-116 2 23     SPACE eurjchem-116 2 24 23 23 NUM eurjchem-116 2 25     SPACE eurjchem-116 2 26 june june PROPN eurjchem-116 2 27     SPACE eurjchem-116 2 28 2010 2010 NUM eurjchem-116 2 29     SPACE eurjchem-116 2 30 accepted accept VERB eurjchem-116 2 31 : : PUNCT eurjchem-116 2 32     SPACE eurjchem-116 2 33 24 24 NUM eurjchem-116 2 34     SPACE eurjchem-116 2 35 june june PROPN eurjchem-116 2 36     SPACE eurjchem-116 2 37 2010 2010 NUM eurjchem-116 2 38     SPACE eurjchem-116 2 39 online online NOUN eurjchem-116 2 40 : : PUNCT eurjchem-116 2 41     SPACE eurjchem-116 2 42 31 31 NUM eurjchem-116 2 43     SPACE eurjchem-116 2 44 december december PROPN eurjchem-116 2 45     SPACE eurjchem-116 2 46 2010 2010 NUM eurjchem-116 2 47     SPACE eurjchem-116 2 48 keywords keyword NOUN eurjchem-116 2 49         SPACE eurjchem-116 2 50 voglibose voglibose NOUN eurjchem-116 2 51     SPACE eurjchem-116 2 52 is be AUX eurjchem-116 2 53     SPACE eurjchem-116 2 54 a a DET eurjchem-116 2 55     SPACE eurjchem-116 2 56 potent potent ADJ eurjchem-116 2 57     SPACE eurjchem-116 2 58 glucosidase glucosidase ADJ eurjchem-116 2 59     SPACE eurjchem-116 2 60 inhibitor inhibitor NOUN eurjchem-116 2 61     SPACE eurjchem-116 2 62 used use VERB eurjchem-116 2 63     SPACE eurjchem-116 2 64 for for ADP eurjchem-116 2 65     SPACE eurjchem-116 2 66 type type NOUN eurjchem-116 2 67     SPACE eurjchem-116 2 68 ii ii NOUN eurjchem-116 2 69     SPACE eurjchem-116 2 70 diabetes diabetes NOUN eurjchem-116 2 71     SPACE eurjchem-116 2 72 mellitus mellitus NOUN eurjchem-116 2 73 . . PUNCT eurjchem-116 2 74     SPACE eurjchem-116 3 1 a a DET eurjchem-116 3 2     SPACE eurjchem-116 3 3 simple simple NOUN eurjchem-116 3 4     SPACE eurjchem-116 3 5 and and CCONJ eurjchem-116 3 6     SPACE eurjchem-116 3 7 rapid rapid ADJ eurjchem-116 3 8     SPACE eurjchem-116 3 9 high high ADJ eurjchem-116 3 10     SPACE eurjchem-116 3 11 performance performance NOUN eurjchem-116 3 12     SPACE eurjchem-116 3 13 liquid liquid NOUN eurjchem-116 3 14     SPACE eurjchem-116 3 15 chromatographic chromatographic ADJ eurjchem-116 3 16     SPACE eurjchem-116 3 17 method method NOUN eurjchem-116 3 18     SPACE eurjchem-116 3 19 with with ADP eurjchem-116 3 20     SPACE eurjchem-116 3 21 refractive refractive ADJ eurjchem-116 3 22     SPACE eurjchem-116 3 23 index index NOUN eurjchem-116 3 24     SPACE eurjchem-116 3 25 detection detection NOUN eurjchem-116 3 26     SPACE eurjchem-116 3 27 was be AUX eurjchem-116 3 28     SPACE eurjchem-116 3 29 developed develop VERB eurjchem-116 3 30     SPACE eurjchem-116 3 31 for for ADP eurjchem-116 3 32     SPACE eurjchem-116 3 33 the the DET eurjchem-116 3 34     SPACE eurjchem-116 3 35 determination determination NOUN eurjchem-116 3 36     SPACE eurjchem-116 3 37 of of ADP eurjchem-116 3 38     SPACE eurjchem-116 3 39 voglibose voglibose NOUN eurjchem-116 3 40     SPACE eurjchem-116 3 41 in in ADP eurjchem-116 3 42     SPACE eurjchem-116 3 43 pharmaceutical pharmaceutical NOUN eurjchem-116 3 44     SPACE eurjchem-116 3 45 formulations formulation NOUN eurjchem-116 3 46 . . PUNCT eurjchem-116 3 47     SPACE eurjchem-116 4 1 development development NOUN eurjchem-116 4 2     SPACE eurjchem-116 4 3 was be AUX eurjchem-116 4 4     SPACE eurjchem-116 4 5 performed perform VERB eurjchem-116 4 6     SPACE eurjchem-116 4 7 on on ADP eurjchem-116 4 8     SPACE eurjchem-116 4 9 a a DET eurjchem-116 4 10     SPACE eurjchem-116 4 11 c18 c18 NOUN eurjchem-116 4 12     SPACE eurjchem-116 4 13 ( ( PUNCT eurjchem-116 4 14 250 250 NUM eurjchem-116 4 15     SPACE eurjchem-116 4 16 x x NOUN eurjchem-116 4 17     SPACE eurjchem-116 4 18 4.6 4.6 NUM eurjchem-116 4 19     SPACE eurjchem-116 4 20 mm mm PROPN eurjchem-116 4 21 , , PUNCT eurjchem-116 4 22     SPACE eurjchem-116 4 23 5 5 NUM eurjchem-116 4 24     SPACE eurjchem-116 4 25 µ µ NUM eurjchem-116 4 26 ) ) PUNCT eurjchem-116 4 27     SPACE eurjchem-116 4 28 column column NOUN eurjchem-116 4 29     SPACE eurjchem-116 4 30 using use VERB eurjchem-116 4 31     SPACE eurjchem-116 4 32 a a DET eurjchem-116 4 33     SPACE eurjchem-116 4 34 mobile mobile ADJ eurjchem-116 4 35     SPACE eurjchem-116 4 36 phase phase NOUN eurjchem-116 4 37     SPACE eurjchem-116 4 38 mixture mixture NOUN eurjchem-116 4 39     SPACE eurjchem-116 4 40 of of ADP eurjchem-116 4 41     SPACE eurjchem-116 4 42 acetonitrile acetonitrile NOUN eurjchem-116 4 43     SPACE eurjchem-116 4 44 and and CCONJ eurjchem-116 4 45     SPACE eurjchem-116 4 46 water water NOUN eurjchem-116 4 47     SPACE eurjchem-116 4 48 in in ADP eurjchem-116 4 49     SPACE eurjchem-116 4 50 the the DET eurjchem-116 4 51     SPACE eurjchem-116 4 52 ratio ratio NOUN eurjchem-116 4 53     SPACE eurjchem-116 4 54 of of ADP eurjchem-116 4 55     SPACE eurjchem-116 4 56 50:50 50:50 NUM eurjchem-116 4 57     SPACE eurjchem-116 4 58 which which PRON eurjchem-116 4 59     SPACE eurjchem-116 4 60 was be AUX eurjchem-116 4 61     SPACE eurjchem-116 4 62 fixed fix VERB eurjchem-116 4 63     SPACE eurjchem-116 4 64 at at ADP eurjchem-116 4 65     SPACE eurjchem-116 4 66 a a DET eurjchem-116 4 67     SPACE eurjchem-116 4 68 flow flow NOUN eurjchem-116 4 69     SPACE eurjchem-116 4 70 rate rate NOUN eurjchem-116 4 71     SPACE eurjchem-116 4 72 of of ADP eurjchem-116 4 73     SPACE eurjchem-116 4 74 0.5 0.5 NUM eurjchem-116 4 75     SPACE eurjchem-116 4 76 ml ml NOUN eurjchem-116 4 77 / / SYM eurjchem-116 4 78 min min NOUN eurjchem-116 4 79 . . PROPN eurjchem-116 4 80     SPACE eurjchem-116 4 81 polarity polarity NOUN eurjchem-116 4 82     SPACE eurjchem-116 4 83 of of ADP eurjchem-116 4 84     SPACE eurjchem-116 4 85 voglibose voglibose NOUN eurjchem-116 4 86     SPACE eurjchem-116 4 87 was be AUX eurjchem-116 4 88     SPACE eurjchem-116 4 89 found find VERB eurjchem-116 4 90     SPACE eurjchem-116 4 91 to to PART eurjchem-116 4 92     SPACE eurjchem-116 4 93 be be AUX eurjchem-116 4 94     SPACE eurjchem-116 4 95 positive positive ADJ eurjchem-116 4 96     SPACE eurjchem-116 4 97 and and CCONJ eurjchem-116 4 98     SPACE eurjchem-116 4 99 elution elution NOUN eurjchem-116 4 100     SPACE eurjchem-116 4 101 time time NOUN eurjchem-116 4 102     SPACE eurjchem-116 4 103 was be AUX eurjchem-116 4 104     SPACE eurjchem-116 4 105 found find VERB eurjchem-116 4 106     SPACE eurjchem-116 4 107 to to PART eurjchem-116 4 108     SPACE eurjchem-116 4 109 be be AUX eurjchem-116 4 110     SPACE eurjchem-116 4 111 less less ADJ eurjchem-116 4 112     SPACE eurjchem-116 4 113 than than ADP eurjchem-116 4 114     SPACE eurjchem-116 4 115 5 5 NUM eurjchem-116 4 116     SPACE eurjchem-116 4 117 min min NOUN eurjchem-116 4 118 . . PROPN eurjchem-116 4 119     SPACE eurjchem-116 4 120 the the DET eurjchem-116 4 121     SPACE eurjchem-116 4 122 method method NOUN eurjchem-116 4 123     SPACE eurjchem-116 4 124 was be AUX eurjchem-116 4 125     SPACE eurjchem-116 4 126 also also ADV eurjchem-116 4 127     SPACE eurjchem-116 4 128 validated validate VERB eurjchem-116 4 129     SPACE eurjchem-116 4 130 as as ADP eurjchem-116 4 131     SPACE eurjchem-116 4 132 per per ADP eurjchem-116 4 133     SPACE eurjchem-116 4 134 ich ich NOUN eurjchem-116 4 135     SPACE eurjchem-116 4 136 guidelines guideline NOUN eurjchem-116 4 137     SPACE eurjchem-116 4 138 for for ADP eurjchem-116 4 139     SPACE eurjchem-116 4 140 its its PRON eurjchem-116 4 141     SPACE eurjchem-116 4 142 linearity linearity NOUN eurjchem-116 4 143 , , PUNCT eurjchem-116 4 144     SPACE eurjchem-116 4 145 precision precision NOUN eurjchem-116 4 146 , , PUNCT eurjchem-116 4 147     SPACE eurjchem-116 4 148 accuracy accuracy NOUN eurjchem-116 4 149     SPACE eurjchem-116 4 150 and and CCONJ eurjchem-116 4 151     SPACE eurjchem-116 4 152 robustness robustness NOUN eurjchem-116 4 153 . . PUNCT eurjchem-116 4 154     SPACE eurjchem-116 5 1 the the DET eurjchem-116 5 2     SPACE eurjchem-116 5 3 limit limit NOUN eurjchem-116 5 4     SPACE eurjchem-116 5 5 of of ADP eurjchem-116 5 6     SPACE eurjchem-116 5 7 detection detection NOUN eurjchem-116 5 8     SPACE eurjchem-116 5 9 and and CCONJ eurjchem-116 5 10     SPACE eurjchem-116 5 11 quantification quantification NOUN eurjchem-116 5 12     SPACE eurjchem-116 5 13 ( ( PUNCT eurjchem-116 5 14 lod lod PROPN eurjchem-116 5 15     SPACE eurjchem-116 5 16 and and CCONJ eurjchem-116 5 17     SPACE eurjchem-116 5 18 loq loq PROPN eurjchem-116 5 19 ) ) PUNCT eurjchem-116 5 20     SPACE eurjchem-116 5 21 were be AUX eurjchem-116 5 22     SPACE eurjchem-116 5 23 found find VERB eurjchem-116 5 24     SPACE eurjchem-116 5 25 to to PART eurjchem-116 5 26     SPACE eurjchem-116 5 27 be be AUX eurjchem-116 5 28     SPACE eurjchem-116 5 29 2.91 2.91 NUM eurjchem-116 5 30     SPACE eurjchem-116 5 31 and and CCONJ eurjchem-116 5 32     SPACE eurjchem-116 5 33 9.7 9.7 NUM eurjchem-116 5 34     SPACE eurjchem-116 5 35 µg µg NOUN eurjchem-116 5 36 / / SYM eurjchem-116 5 37 ml ml NOUN eurjchem-116 5 38 . . PUNCT eurjchem-116 5 39     SPACE eurjchem-116 5 40 the the DET eurjchem-116 5 41     SPACE eurjchem-116 5 42 method method NOUN eurjchem-116 5 43     SPACE eurjchem-116 5 44 could could AUX eurjchem-116 5 45     SPACE eurjchem-116 5 46 be be AUX eurjchem-116 5 47     SPACE eurjchem-116 5 48 successfully successfully ADV eurjchem-116 5 49     SPACE eurjchem-116 5 50 applied apply VERB eurjchem-116 5 51     SPACE eurjchem-116 5 52 for for ADP eurjchem-116 5 53     SPACE eurjchem-116 5 54 the the DET eurjchem-116 5 55     SPACE eurjchem-116 5 56 quantification quantification NOUN eurjchem-116 5 57     SPACE eurjchem-116 5 58 of of ADP eurjchem-116 5 59     SPACE eurjchem-116 5 60 voglibose voglibose NOUN eurjchem-116 5 61     SPACE eurjchem-116 5 62 in in ADP eurjchem-116 5 63     SPACE eurjchem-116 5 64 pharmaceutical pharmaceutical NOUN eurjchem-116 5 65     SPACE eurjchem-116 5 66 formulations formulation NOUN eurjchem-116 5 67 . . PUNCT eurjchem-116 5 68             SPACE eurjchem-116 5 69 voglibose voglibose PROPN eurjchem-116 5 70     SPACE eurjchem-116 5 71 hplc hplc PROPN eurjchem-116 5 72     SPACE eurjchem-116 5 73 rid rid VERB eurjchem-116 5 74     SPACE eurjchem-116 5 75 validation validation NOUN eurjchem-116 5 76     SPACE eurjchem-116 5 77 pharmaceutical pharmaceutical NOUN eurjchem-116 5 78     SPACE eurjchem-116 5 79 formulations formulation NOUN eurjchem-116 5 80         SPACE eurjchem-116 5 81 1 1 NUM eurjchem-116 5 82 . . PUNCT eurjchem-116 5 83     SPACE eurjchem-116 5 84 introduction introduction NOUN eurjchem-116 5 85         SPACE eurjchem-116 5 86 voglibose voglibose NOUN eurjchem-116 5 87     SPACE eurjchem-116 5 88 ( ( PUNCT eurjchem-116 5 89 vgb vgb ADJ eurjchem-116 5 90 ) ) PUNCT eurjchem-116 5 91     SPACE eurjchem-116 5 92 ( ( PUNCT eurjchem-116 5 93 figure figure NOUN eurjchem-116 5 94     SPACE eurjchem-116 5 95 1 1 NUM eurjchem-116 5 96 ) ) PUNCT eurjchem-116 5 97     SPACE eurjchem-116 5 98 a a DET eurjchem-116 5 99     SPACE eurjchem-116 5 100 new new ADJ eurjchem-116 5 101     SPACE eurjchem-116 5 102 potent potent ADJ eurjchem-116 5 103     SPACE eurjchem-116 5 104 glucosidase glucosidase ADJ eurjchem-116 5 105     SPACE eurjchem-116 5 106 inhibitor inhibitor NOUN eurjchem-116 5 107     SPACE eurjchem-116 5 108 used use VERB eurjchem-116 5 109     SPACE eurjchem-116 5 110 for for ADP eurjchem-116 5 111     SPACE eurjchem-116 5 112 type type NOUN eurjchem-116 5 113     SPACE eurjchem-116 5 114 ii ii NOUN eurjchem-116 5 115     SPACE eurjchem-116 5 116 diabetes diabetes NOUN eurjchem-116 5 117     SPACE eurjchem-116 5 118 has have AUX eurjchem-116 5 119     SPACE eurjchem-116 5 120 shown show VERB eurjchem-116 5 121     SPACE eurjchem-116 5 122 strong strong ADJ eurjchem-116 5 123     SPACE eurjchem-116 5 124 anti‐ anti‐ NOUN eurjchem-116 5 125 obesity obesity NOUN eurjchem-116 5 126     SPACE eurjchem-116 5 127 and and CCONJ eurjchem-116 5 128     SPACE eurjchem-116 5 129 anti‐diabetic anti‐diabetic ADJ eurjchem-116 5 130     SPACE eurjchem-116 5 131 activity activity NOUN eurjchem-116 5 132 . . PUNCT eurjchem-116 5 133     SPACE eurjchem-116 6 1 it it PRON eurjchem-116 6 2     SPACE eurjchem-116 6 3 is be AUX eurjchem-116 6 4     SPACE eurjchem-116 6 5 chemically chemically ADV eurjchem-116 6 6     SPACE eurjchem-116 6 7 3,4‐dideoxy‐ 3,4‐dideoxy‐ NUM eurjchem-116 6 8 4‐[[2‐hydroxy‐1‐(hydroxymethyl)ethyl]amino]‐2‐c‐(hydroxyl 4‐[[2‐hydroxy‐1‐(hydroxymethyl)ethyl]amino]‐2‐c‐(hydroxyl NOUN eurjchem-116 6 9     SPACE eurjchem-116 6 10 methyl)‐d‐epiinositol methyl)‐d‐epiinositol NOUN eurjchem-116 6 11 . . PUNCT eurjchem-116 6 12     SPACE eurjchem-116 7 1 it it PRON eurjchem-116 7 2     SPACE eurjchem-116 7 3 was be AUX eurjchem-116 7 4     SPACE eurjchem-116 7 5 found find VERB eurjchem-116 7 6     SPACE eurjchem-116 7 7 that that SCONJ eurjchem-116 7 8     SPACE eurjchem-116 7 9 it it PRON eurjchem-116 7 10     SPACE eurjchem-116 7 11 delays delay VERB eurjchem-116 7 12     SPACE eurjchem-116 7 13 the the DET eurjchem-116 7 14     SPACE eurjchem-116 7 15 glucose glucose NOUN eurjchem-116 7 16     SPACE eurjchem-116 7 17 absorption absorption NOUN eurjchem-116 7 18     SPACE eurjchem-116 7 19 in in ADP eurjchem-116 7 20     SPACE eurjchem-116 7 21 the the DET eurjchem-116 7 22     SPACE eurjchem-116 7 23 gastrointestinal gastrointestinal ADJ eurjchem-116 7 24     SPACE eurjchem-116 7 25 tract tract NOUN eurjchem-116 7 26     SPACE eurjchem-116 7 27 of of ADP eurjchem-116 7 28     SPACE eurjchem-116 7 29 humans human NOUN eurjchem-116 7 30 . . PUNCT eurjchem-116 7 31     SPACE eurjchem-116 7 32 thus thus ADV eurjchem-116 7 33 , , PUNCT eurjchem-116 7 34     SPACE eurjchem-116 7 35 reduces reduce VERB eurjchem-116 7 36     SPACE eurjchem-116 7 37 the the DET eurjchem-116 7 38     SPACE eurjchem-116 7 39 post‐prandial post‐prandial ADJ eurjchem-116 7 40     SPACE eurjchem-116 7 41 blood blood NOUN eurjchem-116 7 42     SPACE eurjchem-116 7 43 glucose glucose NOUN eurjchem-116 7 44     SPACE eurjchem-116 7 45 peaks peak NOUN eurjchem-116 7 46     SPACE eurjchem-116 8 1 [ [ X eurjchem-116 9 1 1–3 1–3 NOUN eurjchem-116 9 2 ] ] X eurjchem-116 9 3 . . PUNCT eurjchem-116 9 4     SPACE eurjchem-116 10 1 voglibose voglibose NOUN eurjchem-116 10 2     SPACE eurjchem-116 10 3 has have VERB eurjchem-116 10 4     SPACE eurjchem-116 10 5 a a DET eurjchem-116 10 6     SPACE eurjchem-116 10 7 structural structural ADJ eurjchem-116 10 8     SPACE eurjchem-116 10 9 relation relation NOUN eurjchem-116 10 10     SPACE eurjchem-116 10 11 with with ADP eurjchem-116 10 12     SPACE eurjchem-116 10 13 natural natural ADJ eurjchem-116 10 14     SPACE eurjchem-116 10 15 carbohydrates carbohydrate NOUN eurjchem-116 10 16     SPACE eurjchem-116 10 17 [ [ X eurjchem-116 10 18 4,5 4,5 NUM eurjchem-116 10 19 ] ] PUNCT eurjchem-116 10 20     SPACE eurjchem-116 10 21 and and CCONJ eurjchem-116 10 22     SPACE eurjchem-116 10 23 are be AUX eurjchem-116 10 24     SPACE eurjchem-116 10 25 present present ADJ eurjchem-116 10 26     SPACE eurjchem-116 10 27 without without ADP eurjchem-116 10 28     SPACE eurjchem-116 10 29 a a DET eurjchem-116 10 30     SPACE eurjchem-116 10 31 chromophore chromophore NOUN eurjchem-116 10 32     SPACE eurjchem-116 10 33 and/or and/or NOUN eurjchem-116 10 34     SPACE eurjchem-116 10 35 fluorophore fluorophore NOUN eurjchem-116 10 36     SPACE eurjchem-116 10 37 groups group NOUN eurjchem-116 10 38     SPACE eurjchem-116 10 39 and and CCONJ eurjchem-116 10 40     SPACE eurjchem-116 10 41 hence hence ADV eurjchem-116 10 42     SPACE eurjchem-116 10 43 does do AUX eurjchem-116 10 44     SPACE eurjchem-116 10 45 not not PART eurjchem-116 10 46     SPACE eurjchem-116 10 47 show show VERB eurjchem-116 10 48     SPACE eurjchem-116 10 49 any any DET eurjchem-116 10 50     SPACE eurjchem-116 10 51 uv uv NOUN eurjchem-116 10 52     SPACE eurjchem-116 10 53 absorbance absorbance NOUN eurjchem-116 10 54 . . PUNCT eurjchem-116 10 55     SPACE eurjchem-116 11 1 the the DET eurjchem-116 11 2     SPACE eurjchem-116 11 3 analysis analysis NOUN eurjchem-116 11 4     SPACE eurjchem-116 11 5 of of ADP eurjchem-116 11 6     SPACE eurjchem-116 11 7 carbohydrates carbohydrate NOUN eurjchem-116 11 8     SPACE eurjchem-116 11 9 has have VERB eurjchem-116 11 10     SPACE eurjchem-116 11 11 an an DET eurjchem-116 11 12     SPACE eurjchem-116 11 13 important important ADJ eurjchem-116 11 14     SPACE eurjchem-116 11 15 role role NOUN eurjchem-116 11 16     SPACE eurjchem-116 11 17 in in ADP eurjchem-116 11 18     SPACE eurjchem-116 11 19 the the DET eurjchem-116 11 20     SPACE eurjchem-116 11 21 pharmaceutical pharmaceutical NOUN eurjchem-116 11 22     SPACE eurjchem-116 11 23 and and CCONJ eurjchem-116 11 24     SPACE eurjchem-116 11 25 food food NOUN eurjchem-116 11 26     SPACE eurjchem-116 11 27 industry industry NOUN eurjchem-116 11 28     SPACE eurjchem-116 11 29 and and CCONJ eurjchem-116 11 30     SPACE eurjchem-116 11 31 their their PRON eurjchem-116 11 32     SPACE eurjchem-116 11 33 analysis analysis NOUN eurjchem-116 11 34     SPACE eurjchem-116 11 35 by by ADP eurjchem-116 11 36     SPACE eurjchem-116 11 37 liquid liquid NOUN eurjchem-116 11 38     SPACE eurjchem-116 11 39 chromatography chromatography NOUN eurjchem-116 11 40     SPACE eurjchem-116 11 41 ( ( PUNCT eurjchem-116 11 42 lc lc PROPN eurjchem-116 11 43 ) ) PUNCT eurjchem-116 11 44     SPACE eurjchem-116 11 45 often often ADV eurjchem-116 11 46     SPACE eurjchem-116 11 47 requires require VERB eurjchem-116 11 48     SPACE eurjchem-116 11 49 derivatization derivatization NOUN eurjchem-116 11 50     SPACE eurjchem-116 11 51 procedures procedure NOUN eurjchem-116 11 52     SPACE eurjchem-116 12 1 [ [ X eurjchem-116 12 2 6 6 NUM eurjchem-116 12 3 ] ] PUNCT eurjchem-116 12 4 . . PUNCT eurjchem-116 12 5     SPACE eurjchem-116 12 6 quantitative quantitative ADJ eurjchem-116 12 7     SPACE eurjchem-116 12 8 determination determination NOUN eurjchem-116 12 9     SPACE eurjchem-116 12 10 of of ADP eurjchem-116 12 11     SPACE eurjchem-116 12 12 voglibose voglibose NOUN eurjchem-116 12 13     SPACE eurjchem-116 12 14 in in ADP eurjchem-116 12 15     SPACE eurjchem-116 12 16 pharmaceutical pharmaceutical NOUN eurjchem-116 12 17     SPACE eurjchem-116 12 18 tablets tablet NOUN eurjchem-116 12 19     SPACE eurjchem-116 12 20 using use VERB eurjchem-116 12 21     SPACE eurjchem-116 12 22 high‐performance high‐performance NOUN eurjchem-116 12 23     SPACE eurjchem-116 12 24 liquid liquid NOUN eurjchem-116 12 25     SPACE eurjchem-116 12 26 chromatography chromatography NOUN eurjchem-116 12 27 – – PUNCT eurjchem-116 12 28 fluorescence fluorescence NOUN eurjchem-116 12 29     SPACE eurjchem-116 12 30 detec‐ detec‐ NOUN eurjchem-116 12 31 tion tion NOUN eurjchem-116 12 32     SPACE eurjchem-116 12 33 with with ADP eurjchem-116 12 34     SPACE eurjchem-116 12 35 post‐column post‐column NOUN eurjchem-116 12 36     SPACE eurjchem-116 12 37 derivatization derivatization NOUN eurjchem-116 12 38     SPACE eurjchem-116 12 39 and and CCONJ eurjchem-116 12 40     SPACE eurjchem-116 12 41 mass mass ADJ eurjchem-116 12 42     SPACE eurjchem-116 12 43 spectrometric spectrometric ADJ eurjchem-116 12 44     SPACE eurjchem-116 12 45 detection detection NOUN eurjchem-116 12 46     SPACE eurjchem-116 12 47 has have AUX eurjchem-116 12 48     SPACE eurjchem-116 12 49 been be AUX eurjchem-116 12 50     SPACE eurjchem-116 12 51 reported report VERB eurjchem-116 12 52     SPACE eurjchem-116 12 53 [ [ X eurjchem-116 12 54 7 7 NUM eurjchem-116 12 55 ] ] PUNCT eurjchem-116 12 56 . . PUNCT eurjchem-116 12 57             SPACE eurjchem-116 12 58 figure figure VERB eurjchem-116 12 59     SPACE eurjchem-116 12 60 1 1 NUM eurjchem-116 12 61 . . PUNCT eurjchem-116 12 62     SPACE eurjchem-116 12 63 structure structure NOUN eurjchem-116 12 64     SPACE eurjchem-116 12 65 of of ADP eurjchem-116 12 66     SPACE eurjchem-116 12 67 voglibose voglibose NOUN eurjchem-116 12 68 . . PUNCT eurjchem-116 12 69     SPACE eurjchem-116 13 1 the the DET eurjchem-116 13 2     SPACE eurjchem-116 13 3 purpose purpose NOUN eurjchem-116 13 4     SPACE eurjchem-116 13 5 of of ADP eurjchem-116 13 6     SPACE eurjchem-116 13 7 this this DET eurjchem-116 13 8     SPACE eurjchem-116 13 9 study study NOUN eurjchem-116 13 10     SPACE eurjchem-116 13 11 was be AUX eurjchem-116 13 12     SPACE eurjchem-116 13 13 to to PART eurjchem-116 13 14     SPACE eurjchem-116 13 15 develop develop VERB eurjchem-116 13 16     SPACE eurjchem-116 13 17 and and CCONJ eurjchem-116 13 18     SPACE eurjchem-116 13 19 validate validate VERB eurjchem-116 13 20     SPACE eurjchem-116 13 21 lc lc PROPN eurjchem-116 13 22 – – PUNCT eurjchem-116 13 23 ri ri NOUN eurjchem-116 13 24     SPACE eurjchem-116 13 25 method method NOUN eurjchem-116 13 26     SPACE eurjchem-116 13 27 for for ADP eurjchem-116 13 28     SPACE eurjchem-116 13 29 the the DET eurjchem-116 13 30     SPACE eurjchem-116 13 31 analysis analysis NOUN eurjchem-116 13 32     SPACE eurjchem-116 13 33 of of ADP eurjchem-116 13 34     SPACE eurjchem-116 13 35 voglibose voglibose NOUN eurjchem-116 13 36     SPACE eurjchem-116 13 37 in in ADP eurjchem-116 13 38     SPACE eurjchem-116 13 39 pharmaceutical pharmaceutical NOUN eurjchem-116 13 40     SPACE eurjchem-116 13 41 formulations formulation NOUN eurjchem-116 13 42 . . PUNCT eurjchem-116 13 43     SPACE eurjchem-116 13 44 to to ADP eurjchem-116 13 45     SPACE eurjchem-116 13 46 our our PRON eurjchem-116 13 47     SPACE eurjchem-116 13 48 knowledge knowledge NOUN eurjchem-116 13 49     SPACE eurjchem-116 13 50 of of ADP eurjchem-116 13 51     SPACE eurjchem-116 13 52 literature literature NOUN eurjchem-116 13 53     SPACE eurjchem-116 13 54 no no DET eurjchem-116 13 55     SPACE eurjchem-116 13 56 lc lc NOUN eurjchem-116 13 57     SPACE eurjchem-116 13 58 method method NOUN eurjchem-116 13 59     SPACE eurjchem-116 13 60 with with ADP eurjchem-116 13 61     SPACE eurjchem-116 13 62 refractive refractive ADJ eurjchem-116 13 63     SPACE eurjchem-116 13 64 index index NOUN eurjchem-116 13 65     SPACE eurjchem-116 13 66 detection detection NOUN eurjchem-116 13 67     SPACE eurjchem-116 13 68 has have AUX eurjchem-116 13 69     SPACE eurjchem-116 13 70 been be AUX eurjchem-116 13 71     SPACE eurjchem-116 13 72 published publish VERB eurjchem-116 13 73     SPACE eurjchem-116 13 74 for for ADP eurjchem-116 13 75     SPACE eurjchem-116 13 76 the the DET eurjchem-116 13 77     SPACE eurjchem-116 13 78 analysis analysis NOUN eurjchem-116 13 79     SPACE eurjchem-116 13 80 of of ADP eurjchem-116 13 81     SPACE eurjchem-116 13 82 voglibose voglibose NOUN eurjchem-116 13 83     SPACE eurjchem-116 13 84 and and CCONJ eurjchem-116 13 85     SPACE eurjchem-116 13 86 could could AUX eurjchem-116 13 87     SPACE eurjchem-116 13 88 be be AUX eurjchem-116 13 89     SPACE eurjchem-116 13 90 successfully successfully ADV eurjchem-116 13 91     SPACE eurjchem-116 13 92 applied apply VERB eurjchem-116 13 93     SPACE eurjchem-116 13 94 to to ADP eurjchem-116 13 95     SPACE eurjchem-116 13 96 the the DET eurjchem-116 13 97     SPACE eurjchem-116 13 98 analysis analysis NOUN eurjchem-116 13 99     SPACE eurjchem-116 13 100 of of ADP eurjchem-116 13 101     SPACE eurjchem-116 13 102 voglibose voglibose NOUN eurjchem-116 13 103     SPACE eurjchem-116 13 104 in in ADP eurjchem-116 13 105     SPACE eurjchem-116 13 106 commercially commercially ADV eurjchem-116 13 107     SPACE eurjchem-116 13 108 available available ADJ eurjchem-116 13 109     SPACE eurjchem-116 13 110 tablets tablet NOUN eurjchem-116 13 111 . . PUNCT eurjchem-116 13 112         SPACE eurjchem-116 14 1 2 2 NUM eurjchem-116 14 2 . . PUNCT eurjchem-116 14 3     SPACE eurjchem-116 14 4 experimental experimental ADJ eurjchem-116 14 5         SPACE eurjchem-116 14 6 2.1 2.1 NUM eurjchem-116 14 7 . . PUNCT eurjchem-116 14 8     SPACE eurjchem-116 14 9 reagents reagent NOUN eurjchem-116 14 10     SPACE eurjchem-116 14 11 and and CCONJ eurjchem-116 14 12     SPACE eurjchem-116 14 13 chemicals chemical NOUN eurjchem-116 14 14         SPACE eurjchem-116 14 15 voglibose voglibose NOUN eurjchem-116 14 16     SPACE eurjchem-116 14 17 was be AUX eurjchem-116 14 18     SPACE eurjchem-116 14 19 obtained obtain VERB eurjchem-116 14 20     SPACE eurjchem-116 14 21 from from ADP eurjchem-116 14 22     SPACE eurjchem-116 14 23 ranbaxy ranbaxy PROPN eurjchem-116 14 24     SPACE eurjchem-116 14 25 research research NOUN eurjchem-116 14 26     SPACE eurjchem-116 14 27 laboratories laboratory NOUN eurjchem-116 14 28 , , PUNCT eurjchem-116 14 29     SPACE eurjchem-116 14 30 india india PROPN eurjchem-116 14 31 . . PUNCT eurjchem-116 14 32     SPACE eurjchem-116 15 1 acetonitrile acetonitrile NOUN eurjchem-116 15 2     SPACE eurjchem-116 15 3 and and CCONJ eurjchem-116 15 4     SPACE eurjchem-116 15 5 methanol methanol NOUN eurjchem-116 15 6     SPACE eurjchem-116 15 7 ( ( PUNCT eurjchem-116 15 8 hplc hplc NOUN eurjchem-116 15 9     SPACE eurjchem-116 15 10 grade grade NOUN eurjchem-116 15 11 ) ) PUNCT eurjchem-116 15 12     SPACE eurjchem-116 15 13 purchased purchase VERB eurjchem-116 15 14     SPACE eurjchem-116 15 15 from from ADP eurjchem-116 15 16     SPACE eurjchem-116 15 17 rankem rankem PROPN eurjchem-116 15 18     SPACE eurjchem-116 15 19 ltd ltd PROPN eurjchem-116 15 20 , , PUNCT eurjchem-116 15 21     SPACE eurjchem-116 15 22 new new ADJ eurjchem-116 15 23     SPACE eurjchem-116 15 24 delhi delhi ADJ eurjchem-116 15 25 , , PUNCT eurjchem-116 15 26     SPACE eurjchem-116 15 27 india india PROPN eurjchem-116 15 28 . . PUNCT eurjchem-116 15 29     SPACE eurjchem-116 15 30 aqueous aqueous ADJ eurjchem-116 15 31     SPACE eurjchem-116 15 32 solutions solution NOUN eurjchem-116 15 33     SPACE eurjchem-116 15 34 were be AUX eurjchem-116 15 35     SPACE eurjchem-116 15 36 prepared prepare VERB eurjchem-116 15 37     SPACE eurjchem-116 15 38 by by ADP eurjchem-116 15 39     SPACE eurjchem-116 15 40 using use VERB eurjchem-116 15 41     SPACE eurjchem-116 15 42 milli milli NOUN eurjchem-116 15 43     SPACE eurjchem-116 15 44 q q NOUN eurjchem-116 15 45     SPACE eurjchem-116 15 46 ( ( PUNCT eurjchem-116 15 47 millipore millipore PROPN eurjchem-116 15 48 , , PUNCT eurjchem-116 15 49     SPACE eurjchem-116 15 50 usa usa PROPN eurjchem-116 15 51 ) ) PUNCT eurjchem-116 15 52     SPACE eurjchem-116 15 53 grade grade NOUN eurjchem-116 15 54     SPACE eurjchem-116 15 55 water water NOUN eurjchem-116 15 56     SPACE eurjchem-116 15 57 and and CCONJ eurjchem-116 15 58     SPACE eurjchem-116 15 59 all all PRON eurjchem-116 15 60     SPACE eurjchem-116 15 61 the the DET eurjchem-116 15 62     SPACE eurjchem-116 15 63 other other ADJ eurjchem-116 15 64     SPACE eurjchem-116 15 65 reagents reagent NOUN eurjchem-116 15 66     SPACE eurjchem-116 15 67 used use VERB eurjchem-116 15 68     SPACE eurjchem-116 15 69 were be AUX eurjchem-116 15 70     SPACE eurjchem-116 15 71 of of ADP eurjchem-116 15 72     SPACE eurjchem-116 15 73 analytical analytical ADJ eurjchem-116 15 74     SPACE eurjchem-116 15 75 reagent reagent ADJ eurjchem-116 15 76     SPACE eurjchem-116 15 77 grade grade NOUN eurjchem-116 15 78 . . PUNCT eurjchem-116 15 79         SPACE eurjchem-116 16 1 2.2 2.2 NUM eurjchem-116 16 2 . . PUNCT eurjchem-116 16 3     SPACE eurjchem-116 16 4 chromatography chromatography NOUN eurjchem-116 16 5         SPACE eurjchem-116 16 6 the the DET eurjchem-116 16 7     SPACE eurjchem-116 16 8 hplc hplc NOUN eurjchem-116 16 9     SPACE eurjchem-116 16 10 system system NOUN eurjchem-116 16 11     SPACE eurjchem-116 16 12 consisted consist VERB eurjchem-116 16 13     SPACE eurjchem-116 16 14 of of ADP eurjchem-116 16 15     SPACE eurjchem-116 16 16 shimadzu shimadzu VERB eurjchem-116 16 17     SPACE eurjchem-116 16 18 cbm‐20a cbm‐20a VERB eurjchem-116 16 19     SPACE eurjchem-116 16 20 prominence prominence NOUN eurjchem-116 16 21     SPACE eurjchem-116 16 22 communication communication NOUN eurjchem-116 16 23     SPACE eurjchem-116 16 24 bus bus NOUN eurjchem-116 16 25     SPACE eurjchem-116 16 26 module module NOUN eurjchem-116 16 27     SPACE eurjchem-116 16 28 with with ADP eurjchem-116 16 29     SPACE eurjchem-116 16 30 dgu‐20a5 dgu‐20a5 PROPN eurjchem-116 16 31     SPACE eurjchem-116 16 32 prominence prominence NOUN eurjchem-116 16 33     SPACE eurjchem-116 16 34 degasser degasser PROPN eurjchem-116 16 35     SPACE eurjchem-116 16 36 and and CCONJ eurjchem-116 16 37     SPACE eurjchem-116 16 38 sil‐10advp sil‐10advp PROPN eurjchem-116 16 39     SPACE eurjchem-116 16 40 auto auto NOUN eurjchem-116 16 41     SPACE eurjchem-116 16 42 injector injector NOUN eurjchem-116 16 43     SPACE eurjchem-116 16 44 connected connect VERB eurjchem-116 16 45     SPACE eurjchem-116 16 46 to to ADP eurjchem-116 16 47     SPACE eurjchem-116 16 48 a a DET eurjchem-116 16 49     SPACE eurjchem-116 16 50 rid‐10a rid‐10a NOUN eurjchem-116 16 51     SPACE eurjchem-116 16 52 refractive refractive ADJ eurjchem-116 16 53     SPACE eurjchem-116 16 54 index index NOUN eurjchem-116 16 55     SPACE eurjchem-116 16 56 detector detector NOUN eurjchem-116 16 57 . . PUNCT eurjchem-116 16 58     SPACE eurjchem-116 17 1 the the DET eurjchem-116 17 2     SPACE eurjchem-116 17 3 data datum NOUN eurjchem-116 17 4     SPACE eurjchem-116 17 5 were be AUX eurjchem-116 17 6     SPACE eurjchem-116 17 7 acquired acquire VERB eurjchem-116 17 8     SPACE eurjchem-116 17 9 and and CCONJ eurjchem-116 17 10     SPACE eurjchem-116 17 11 processed process VERB eurjchem-116 17 12     SPACE eurjchem-116 17 13 with with ADP eurjchem-116 17 14     SPACE eurjchem-116 17 15 lc lc NOUN eurjchem-116 17 16     SPACE eurjchem-116 17 17 solution solution NOUN eurjchem-116 17 18     SPACE eurjchem-116 17 19 version version NOUN eurjchem-116 17 20     SPACE eurjchem-116 17 21 1.22 1.22 NUM eurjchem-116 17 22     SPACE eurjchem-116 17 23 sp1 sp1 NOUN eurjchem-116 17 24     SPACE eurjchem-116 17 25 software software NOUN eurjchem-116 17 26 . . PUNCT eurjchem-116 17 27     SPACE eurjchem-116 18 1 the the DET eurjchem-116 18 2     SPACE eurjchem-116 18 3 analytical analytical ADJ eurjchem-116 18 4     SPACE eurjchem-116 18 5 column column NOUN eurjchem-116 18 6     SPACE eurjchem-116 18 7 was be AUX eurjchem-116 18 8     SPACE eurjchem-116 18 9 a a DET eurjchem-116 18 10     SPACE eurjchem-116 18 11 waters water NOUN eurjchem-116 18 12     SPACE eurjchem-116 18 13 c18 c18 NOUN eurjchem-116 18 14 , , PUNCT eurjchem-116 18 15     SPACE eurjchem-116 18 16 with with ADP eurjchem-116 18 17     SPACE eurjchem-116 18 18 4.6 4.6 NUM eurjchem-116 18 19     SPACE eurjchem-116 18 20 x x NOUN eurjchem-116 18 21     SPACE eurjchem-116 18 22 250 250 NUM eurjchem-116 18 23     SPACE eurjchem-116 18 24 mm mm PROPN eurjchem-116 18 25 , , PUNCT eurjchem-116 18 26     SPACE eurjchem-116 18 27 5 5 NUM eurjchem-116 18 28     SPACE eurjchem-116 18 29 µm µm NOUN eurjchem-116 18 30     SPACE eurjchem-116 18 31 particle particle NOUN eurjchem-116 18 32     SPACE eurjchem-116 18 33 size size NOUN eurjchem-116 18 34 . . PUNCT eurjchem-116 18 35     SPACE eurjchem-116 19 1 the the DET eurjchem-116 19 2     SPACE eurjchem-116 19 3 isocratic isocratic ADJ eurjchem-116 19 4     SPACE eurjchem-116 19 5 mobile mobile ADJ eurjchem-116 19 6     SPACE eurjchem-116 19 7 phase phase NOUN eurjchem-116 19 8     SPACE eurjchem-116 19 9 consisted consist VERB eurjchem-116 19 10     SPACE eurjchem-116 19 11 of of ADP eurjchem-116 19 12     SPACE eurjchem-116 19 13 acetonitrile acetonitrile NOUN eurjchem-116 19 14     SPACE eurjchem-116 19 15 and and CCONJ eurjchem-116 19 16     SPACE eurjchem-116 19 17 water water NOUN eurjchem-116 19 18     SPACE eurjchem-116 19 19 mixture mixture NOUN eurjchem-116 19 20     SPACE eurjchem-116 19 21 ( ( PUNCT eurjchem-116 19 22 50:50 50:50 NUM eurjchem-116 19 23 , , PUNCT eurjchem-116 19 24     SPACE eurjchem-116 19 25 v v ADJ eurjchem-116 19 26 : : PUNCT eurjchem-116 19 27 v v NOUN eurjchem-116 19 28 ) ) PUNCT eurjchem-116 19 29     SPACE eurjchem-116 19 30 was be AUX eurjchem-116 19 31     SPACE eurjchem-116 19 32 run run VERB eurjchem-116 19 33     SPACE eurjchem-116 19 34 at at ADP eurjchem-116 19 35     SPACE eurjchem-116 19 36 a a DET eurjchem-116 19 37     SPACE eurjchem-116 19 38 flow flow NOUN eurjchem-116 19 39     SPACE eurjchem-116 19 40 rate rate NOUN eurjchem-116 19 41     SPACE eurjchem-116 19 42 of of ADP eurjchem-116 19 43     SPACE eurjchem-116 19 44 0.5 0.5 NUM eurjchem-116 19 45     SPACE eurjchem-116 19 46 ml ml NOUN eurjchem-116 19 47 / / SYM eurjchem-116 19 48 min min NOUN eurjchem-116 19 49 . . PROPN eurjchem-116 19 50     SPACE eurjchem-116 19 51 the the DET eurjchem-116 19 52     SPACE eurjchem-116 19 53 cell cell NOUN eurjchem-116 19 54     SPACE eurjchem-116 19 55 temperature temperature NOUN eurjchem-116 19 56     SPACE eurjchem-116 19 57 was be AUX eurjchem-116 19 58     SPACE eurjchem-116 19 59 maintained maintain VERB eurjchem-116 19 60     SPACE eurjchem-116 19 61 at at ADP eurjchem-116 19 62     SPACE eurjchem-116 19 63 40 40 NUM eurjchem-116 19 64     SPACE eurjchem-116 19 65 oc oc PROPN eurjchem-116 19 66 . . PUNCT eurjchem-116 19 67         SPACE eurjchem-116 19 68 2.3 2.3 NUM eurjchem-116 19 69 . . PUNCT eurjchem-116 19 70     SPACE eurjchem-116 19 71 standard standard ADJ eurjchem-116 19 72     SPACE eurjchem-116 19 73 solutions solution NOUN eurjchem-116 19 74         SPACE eurjchem-116 19 75 stock stock NOUN eurjchem-116 19 76     SPACE eurjchem-116 19 77 standard standard ADJ eurjchem-116 19 78     SPACE eurjchem-116 19 79 solution solution NOUN eurjchem-116 19 80     SPACE eurjchem-116 19 81 of of ADP eurjchem-116 19 82     SPACE eurjchem-116 19 83 voglibose voglibose NOUN eurjchem-116 19 84     SPACE eurjchem-116 19 85 was be AUX eurjchem-116 19 86     SPACE eurjchem-116 19 87 prepared prepare VERB eurjchem-116 19 88     SPACE eurjchem-116 19 89 by by ADP eurjchem-116 19 90     SPACE eurjchem-116 19 91 taking take VERB eurjchem-116 19 92     SPACE eurjchem-116 19 93 25 25 NUM eurjchem-116 19 94     SPACE eurjchem-116 19 95 mg mg NOUN eurjchem-116 19 96     SPACE eurjchem-116 19 97 of of ADP eurjchem-116 19 98     SPACE eurjchem-116 19 99 the the DET eurjchem-116 19 100     SPACE eurjchem-116 19 101 drug drug NOUN eurjchem-116 19 102     SPACE eurjchem-116 19 103 in in ADP eurjchem-116 19 104     SPACE eurjchem-116 19 105 a a DET eurjchem-116 19 106     SPACE eurjchem-116 19 107 25 25 NUM eurjchem-116 19 108     SPACE eurjchem-116 19 109 ml ml NOUN eurjchem-116 19 110     SPACE eurjchem-116 19 111 volumetric volumetric NOUN eurjchem-116 19 112     SPACE eurjchem-116 19 113 flask flask NOUN eurjchem-116 19 114     SPACE eurjchem-116 19 115 to to ADP eurjchem-116 19 116     SPACE eurjchem-116 19 117 final final ADJ eurjchem-116 19 118     SPACE eurjchem-116 19 119 lakshmi lakshmi NOUN eurjchem-116 19 120     SPACE eurjchem-116 19 121 and and CCONJ eurjchem-116 19 122     SPACE eurjchem-116 19 123 rajesh rajesh PROPN eurjchem-116 19 124     SPACE eurjchem-116 19 125 / / SYM eurjchem-116 19 126     SPACE eurjchem-116 19 127 european european ADJ eurjchem-116 19 128     SPACE eurjchem-116 19 129 journal journal NOUN eurjchem-116 19 130     SPACE eurjchem-116 19 131 of of ADP eurjchem-116 19 132     SPACE eurjchem-116 19 133 chemistry chemistry NOUN eurjchem-116 19 134     SPACE eurjchem-116 19 135 1 1 NUM eurjchem-116 19 136     SPACE eurjchem-116 19 137 ( ( PUNCT eurjchem-116 19 138 4 4 NUM eurjchem-116 19 139 ) ) PUNCT eurjchem-116 19 140     SPACE eurjchem-116 19 141 ( ( PUNCT eurjchem-116 19 142 2010 2010 NUM eurjchem-116 19 143 ) ) PUNCT eurjchem-116 19 144     SPACE eurjchem-116 19 145 262­265 262­265 NOUN eurjchem-116 19 146     SPACE eurjchem-116 19 147 263 263 NUM eurjchem-116 19 148     SPACE eurjchem-116 19 149 concentration concentration NOUN eurjchem-116 19 150     SPACE eurjchem-116 19 151 of of ADP eurjchem-116 19 152     SPACE eurjchem-116 19 153 1 1 NUM eurjchem-116 19 154     SPACE eurjchem-116 19 155 mg mg PROPN eurjchem-116 19 156 / / SYM eurjchem-116 19 157 ml ml NOUN eurjchem-116 19 158 , , PUNCT eurjchem-116 19 159     SPACE eurjchem-116 19 160 and and CCONJ eurjchem-116 19 161     SPACE eurjchem-116 19 162 working work VERB eurjchem-116 19 163     SPACE eurjchem-116 19 164 standard standard ADJ eurjchem-116 19 165     SPACE eurjchem-116 19 166 solution solution NOUN eurjchem-116 19 167     SPACE eurjchem-116 19 168 of of ADP eurjchem-116 19 169     SPACE eurjchem-116 19 170 100 100 NUM eurjchem-116 19 171     SPACE eurjchem-116 19 172 µg µg VERB eurjchem-116 19 173 / / SYM eurjchem-116 19 174 ml ml VERB eurjchem-116 19 175     SPACE eurjchem-116 19 176 was be AUX eurjchem-116 19 177     SPACE eurjchem-116 19 178 prepared prepare VERB eurjchem-116 19 179     SPACE eurjchem-116 19 180 by by ADP eurjchem-116 19 181     SPACE eurjchem-116 19 182 diluting dilute VERB eurjchem-116 19 183     SPACE eurjchem-116 19 184 1 1 NUM eurjchem-116 19 185     SPACE eurjchem-116 19 186 ml ml NOUN eurjchem-116 19 187     SPACE eurjchem-116 19 188 of of ADP eurjchem-116 19 189     SPACE eurjchem-116 19 190 the the DET eurjchem-116 19 191     SPACE eurjchem-116 19 192 stock stock NOUN eurjchem-116 19 193     SPACE eurjchem-116 19 194 standard standard ADJ eurjchem-116 19 195     SPACE eurjchem-116 19 196 solution solution NOUN eurjchem-116 19 197     SPACE eurjchem-116 19 198 with with ADP eurjchem-116 19 199     SPACE eurjchem-116 19 200 the the DET eurjchem-116 19 201     SPACE eurjchem-116 19 202 mobile mobile ADJ eurjchem-116 19 203     SPACE eurjchem-116 19 204 phase phase NOUN eurjchem-116 19 205     SPACE eurjchem-116 19 206 to to ADP eurjchem-116 19 207     SPACE eurjchem-116 19 208 10 10 NUM eurjchem-116 19 209     SPACE eurjchem-116 19 210 ml ml NOUN eurjchem-116 19 211 . . PUNCT eurjchem-116 19 212         SPACE eurjchem-116 19 213 2.4 2.4 NUM eurjchem-116 19 214 . . PUNCT eurjchem-116 19 215     SPACE eurjchem-116 19 216 preparation preparation NOUN eurjchem-116 19 217     SPACE eurjchem-116 19 218 of of ADP eurjchem-116 19 219     SPACE eurjchem-116 19 220 the the DET eurjchem-116 19 221     SPACE eurjchem-116 19 222 tablet tablet NOUN eurjchem-116 19 223     SPACE eurjchem-116 19 224 sample sample NOUN eurjchem-116 19 225         SPACE eurjchem-116 19 226 twenty twenty NUM eurjchem-116 19 227     SPACE eurjchem-116 19 228 tablets tablet NOUN eurjchem-116 19 229     SPACE eurjchem-116 19 230 were be AUX eurjchem-116 19 231     SPACE eurjchem-116 19 232 finely finely ADV eurjchem-116 19 233     SPACE eurjchem-116 19 234 powdered powder VERB eurjchem-116 19 235     SPACE eurjchem-116 19 236 and and CCONJ eurjchem-116 19 237     SPACE eurjchem-116 19 238 quantity quantity NOUN eurjchem-116 19 239     SPACE eurjchem-116 19 240 equivalent equivalent NOUN eurjchem-116 19 241     SPACE eurjchem-116 19 242 to to ADP eurjchem-116 19 243     SPACE eurjchem-116 19 244 one one NUM eurjchem-116 19 245     SPACE eurjchem-116 19 246 tablet tablet NOUN eurjchem-116 19 247     SPACE eurjchem-116 19 248 was be AUX eurjchem-116 19 249     SPACE eurjchem-116 19 250 accurately accurately ADV eurjchem-116 19 251     SPACE eurjchem-116 19 252 weighed weigh VERB eurjchem-116 19 253     SPACE eurjchem-116 19 254 and and CCONJ eurjchem-116 19 255     SPACE eurjchem-116 19 256 extracted extract VERB eurjchem-116 19 257     SPACE eurjchem-116 19 258 with with ADP eurjchem-116 19 259     SPACE eurjchem-116 19 260 100 100 NUM eurjchem-116 19 261     SPACE eurjchem-116 19 262 ml ml NOUN eurjchem-116 19 263     SPACE eurjchem-116 19 264 of of ADP eurjchem-116 19 265     SPACE eurjchem-116 19 266 the the DET eurjchem-116 19 267     SPACE eurjchem-116 19 268 mobile mobile ADJ eurjchem-116 19 269     SPACE eurjchem-116 19 270 phase phase NOUN eurjchem-116 19 271 . . PUNCT eurjchem-116 19 272     SPACE eurjchem-116 20 1 it it PRON eurjchem-116 20 2     SPACE eurjchem-116 20 3 was be AUX eurjchem-116 20 4     SPACE eurjchem-116 20 5 sonicated sonicate VERB eurjchem-116 20 6     SPACE eurjchem-116 20 7 for for ADP eurjchem-116 20 8     SPACE eurjchem-116 20 9 30 30 NUM eurjchem-116 20 10     SPACE eurjchem-116 20 11 min min NOUN eurjchem-116 20 12     SPACE eurjchem-116 20 13 with with ADP eurjchem-116 20 14     SPACE eurjchem-116 20 15 vortex vortex NOUN eurjchem-116 20 16     SPACE eurjchem-116 20 17 mixing mixing NOUN eurjchem-116 20 18     SPACE eurjchem-116 20 19 at at ADP eurjchem-116 20 20     SPACE eurjchem-116 20 21 10 10 NUM eurjchem-116 20 22     SPACE eurjchem-116 20 23 min min NOUN eurjchem-116 20 24     SPACE eurjchem-116 20 25 intervals interval NOUN eurjchem-116 20 26     SPACE eurjchem-116 20 27 to to PART eurjchem-116 20 28     SPACE eurjchem-116 20 29 avoid avoid VERB eurjchem-116 20 30     SPACE eurjchem-116 20 31 aggregation aggregation NOUN eurjchem-116 20 32     SPACE eurjchem-116 20 33 of of ADP eurjchem-116 20 34     SPACE eurjchem-116 20 35 the the DET eurjchem-116 20 36     SPACE eurjchem-116 20 37 powdered powdered ADJ eurjchem-116 20 38     SPACE eurjchem-116 20 39 samples sample NOUN eurjchem-116 20 40 . . PUNCT eurjchem-116 20 41     SPACE eurjchem-116 20 42 after after ADP eurjchem-116 20 43     SPACE eurjchem-116 20 44 centrifugation centrifugation NOUN eurjchem-116 20 45     SPACE eurjchem-116 20 46 ( ( PUNCT eurjchem-116 20 47 2000 2000 NUM eurjchem-116 20 48     SPACE eurjchem-116 20 49 × × NOUN eurjchem-116 20 50     SPACE eurjchem-116 20 51 g g NOUN eurjchem-116 20 52     SPACE eurjchem-116 20 53 for for ADP eurjchem-116 20 54     SPACE eurjchem-116 20 55 10 10 NUM eurjchem-116 20 56     SPACE eurjchem-116 20 57 min min NOUN eurjchem-116 20 58 ) ) PUNCT eurjchem-116 20 59 , , PUNCT eurjchem-116 20 60     SPACE eurjchem-116 20 61 10 10 NUM eurjchem-116 20 62     SPACE eurjchem-116 20 63 ml ml NOUN eurjchem-116 20 64     SPACE eurjchem-116 20 65 of of ADP eurjchem-116 20 66     SPACE eurjchem-116 20 67 supernatant supernatant NOUN eurjchem-116 20 68     SPACE eurjchem-116 20 69 was be AUX eurjchem-116 20 70     SPACE eurjchem-116 20 71 collected collect VERB eurjchem-116 20 72     SPACE eurjchem-116 20 73 and and CCONJ eurjchem-116 20 74     SPACE eurjchem-116 20 75 diluted dilute VERB eurjchem-116 20 76     SPACE eurjchem-116 20 77 in in ADP eurjchem-116 20 78     SPACE eurjchem-116 20 79 a a DET eurjchem-116 20 80     SPACE eurjchem-116 20 81 50 50 NUM eurjchem-116 20 82     SPACE eurjchem-116 20 83 ml ml NOUN eurjchem-116 20 84     SPACE eurjchem-116 20 85 volumetric volumetric NOUN eurjchem-116 20 86     SPACE eurjchem-116 20 87 flask flask NOUN eurjchem-116 20 88     SPACE eurjchem-116 20 89 with with ADP eurjchem-116 20 90     SPACE eurjchem-116 20 91 the the DET eurjchem-116 20 92     SPACE eurjchem-116 20 93 mobile mobile ADJ eurjchem-116 20 94     SPACE eurjchem-116 20 95 phase phase NOUN eurjchem-116 20 96     SPACE eurjchem-116 20 97 in in ADP eurjchem-116 20 98     SPACE eurjchem-116 20 99 order order NOUN eurjchem-116 20 100     SPACE eurjchem-116 20 101 to to PART eurjchem-116 20 102     SPACE eurjchem-116 20 103 obtain obtain VERB eurjchem-116 20 104     SPACE eurjchem-116 20 105 a a DET eurjchem-116 20 106     SPACE eurjchem-116 20 107 final final ADJ eurjchem-116 20 108     SPACE eurjchem-116 20 109 concentrations concentration NOUN eurjchem-116 20 110     SPACE eurjchem-116 20 111 of of ADP eurjchem-116 20 112     SPACE eurjchem-116 20 113 20 20 NUM eurjchem-116 20 114     SPACE eurjchem-116 20 115 and and CCONJ eurjchem-116 20 116     SPACE eurjchem-116 20 117 30 30 NUM eurjchem-116 20 118     SPACE eurjchem-116 20 119 µg µg NOUN eurjchem-116 20 120 / / SYM eurjchem-116 20 121 ml ml NOUN eurjchem-116 20 122 . . PUNCT eurjchem-116 20 123     SPACE eurjchem-116 20 124 these these DET eurjchem-116 20 125     SPACE eurjchem-116 20 126 solutions solution NOUN eurjchem-116 20 127     SPACE eurjchem-116 20 128 were be AUX eurjchem-116 20 129     SPACE eurjchem-116 20 130 then then ADV eurjchem-116 20 131     SPACE eurjchem-116 20 132 filtered filter VERB eurjchem-116 20 133     SPACE eurjchem-116 20 134 through through ADP eurjchem-116 20 135     SPACE eurjchem-116 20 136 a a DET eurjchem-116 20 137     SPACE eurjchem-116 20 138 0.22 0.22 NUM eurjchem-116 20 139     SPACE eurjchem-116 20 140 µm µm NOUN eurjchem-116 20 141     SPACE eurjchem-116 20 142 filter filter NOUN eurjchem-116 20 143     SPACE eurjchem-116 20 144 and and CCONJ eurjchem-116 20 145     SPACE eurjchem-116 20 146 injected inject VERB eurjchem-116 20 147     SPACE eurjchem-116 20 148 into into ADP eurjchem-116 20 149     SPACE eurjchem-116 20 150 hplc hplc NOUN eurjchem-116 20 151     SPACE eurjchem-116 20 152 system system NOUN eurjchem-116 20 153 . . PUNCT eurjchem-116 20 154         SPACE eurjchem-116 21 1 2.5 2.5 NUM eurjchem-116 21 2 . . PUNCT eurjchem-116 21 3     SPACE eurjchem-116 22 1 validation validation NOUN eurjchem-116 22 2         SPACE eurjchem-116 22 3 the the DET eurjchem-116 22 4     SPACE eurjchem-116 22 5 validation validation NOUN eurjchem-116 22 6     SPACE eurjchem-116 22 7 of of ADP eurjchem-116 22 8     SPACE eurjchem-116 22 9 an an DET eurjchem-116 22 10     SPACE eurjchem-116 22 11 analytical analytical ADJ eurjchem-116 22 12     SPACE eurjchem-116 22 13 method method NOUN eurjchem-116 22 14     SPACE eurjchem-116 22 15 verifies verifie NOUN eurjchem-116 22 16     SPACE eurjchem-116 22 17 that that SCONJ eurjchem-116 22 18     SPACE eurjchem-116 22 19 the the DET eurjchem-116 22 20     SPACE eurjchem-116 22 21 characteristics characteristic NOUN eurjchem-116 22 22     SPACE eurjchem-116 22 23 of of ADP eurjchem-116 22 24     SPACE eurjchem-116 22 25 the the DET eurjchem-116 22 26     SPACE eurjchem-116 22 27 method method NOUN eurjchem-116 22 28     SPACE eurjchem-116 22 29 satisfy satisfy VERB eurjchem-116 22 30     SPACE eurjchem-116 22 31 the the DET eurjchem-116 22 32     SPACE eurjchem-116 22 33 requirements requirement NOUN eurjchem-116 22 34     SPACE eurjchem-116 22 35 of of ADP eurjchem-116 22 36     SPACE eurjchem-116 22 37 the the DET eurjchem-116 22 38     SPACE eurjchem-116 22 39 application application NOUN eurjchem-116 22 40     SPACE eurjchem-116 22 41 domain domain NOUN eurjchem-116 22 42     SPACE eurjchem-116 22 43 [ [ X eurjchem-116 22 44 8 8 NUM eurjchem-116 22 45 ] ] PUNCT eurjchem-116 22 46 . . PUNCT eurjchem-116 22 47     SPACE eurjchem-116 23 1 the the DET eurjchem-116 23 2     SPACE eurjchem-116 23 3 proposed propose VERB eurjchem-116 23 4     SPACE eurjchem-116 23 5 method method NOUN eurjchem-116 23 6     SPACE eurjchem-116 23 7 was be AUX eurjchem-116 23 8     SPACE eurjchem-116 23 9 validated validate VERB eurjchem-116 23 10     SPACE eurjchem-116 23 11 in in ADP eurjchem-116 23 12     SPACE eurjchem-116 23 13 the the DET eurjchem-116 23 14     SPACE eurjchem-116 23 15 light light NOUN eurjchem-116 23 16     SPACE eurjchem-116 23 17 of of ADP eurjchem-116 23 18     SPACE eurjchem-116 23 19 ich ich NOUN eurjchem-116 23 20     SPACE eurjchem-116 23 21 guidelines guideline VERB eurjchem-116 23 22     SPACE eurjchem-116 24 1 [ [ X eurjchem-116 24 2 9,10 9,10 NUM eurjchem-116 24 3 ] ] X eurjchem-116 24 4     SPACE eurjchem-116 24 5 for for ADP eurjchem-116 24 6     SPACE eurjchem-116 24 7 linearity linearity NOUN eurjchem-116 24 8 , , PUNCT eurjchem-116 24 9     SPACE eurjchem-116 24 10 intra‐ intra‐ NOUN eurjchem-116 24 11     SPACE eurjchem-116 24 12 and and CCONJ eurjchem-116 24 13     SPACE eurjchem-116 24 14 inter‐ inter‐ NOUN eurjchem-116 24 15 day day NOUN eurjchem-116 24 16     SPACE eurjchem-116 24 17 precision precision NOUN eurjchem-116 24 18 , , PUNCT eurjchem-116 24 19     SPACE eurjchem-116 24 20 lod lod PROPN eurjchem-116 24 21 , , PUNCT eurjchem-116 24 22     SPACE eurjchem-116 24 23 loq loq PROPN eurjchem-116 24 24 , , PUNCT eurjchem-116 24 25     SPACE eurjchem-116 24 26 selectivity selectivity NOUN eurjchem-116 24 27     SPACE eurjchem-116 24 28 and and CCONJ eurjchem-116 24 29     SPACE eurjchem-116 24 30 specificity specificity NOUN eurjchem-116 24 31 , , PUNCT eurjchem-116 24 32     SPACE eurjchem-116 24 33 stability stability NOUN eurjchem-116 24 34     SPACE eurjchem-116 24 35 and and CCONJ eurjchem-116 24 36     SPACE eurjchem-116 24 37 recovery recovery NOUN eurjchem-116 24 38 . . PUNCT eurjchem-116 24 39     SPACE eurjchem-116 25 1 consequently consequently ADV eurjchem-116 25 2 , , PUNCT eurjchem-116 25 3     SPACE eurjchem-116 25 4 the the DET eurjchem-116 25 5     SPACE eurjchem-116 25 6 following following NOUN eurjchem-116 25 7     SPACE eurjchem-116 25 8 were be AUX eurjchem-116 25 9     SPACE eurjchem-116 25 10 performed perform VERB eurjchem-116 25 11 . . PUNCT eurjchem-116 25 12         SPACE eurjchem-116 26 1 2.5.1 2.5.1 NUM eurjchem-116 26 2 . . PUNCT eurjchem-116 26 3     SPACE eurjchem-116 26 4 linearity linearity NOUN eurjchem-116 26 5     SPACE eurjchem-116 26 6 and and CCONJ eurjchem-116 26 7     SPACE eurjchem-116 26 8 calibration calibration NOUN eurjchem-116 26 9     SPACE eurjchem-116 26 10 curve curve NOUN eurjchem-116 26 11         SPACE eurjchem-116 26 12 calibration calibration NOUN eurjchem-116 26 13     SPACE eurjchem-116 26 14 curve curve NOUN eurjchem-116 26 15     SPACE eurjchem-116 26 16 of of ADP eurjchem-116 26 17     SPACE eurjchem-116 26 18 peak peak NOUN eurjchem-116 26 19     SPACE eurjchem-116 26 20 area area NOUN eurjchem-116 26 21     SPACE eurjchem-116 26 22 as as ADP eurjchem-116 26 23     SPACE eurjchem-116 26 24 a a DET eurjchem-116 26 25     SPACE eurjchem-116 26 26 function function NOUN eurjchem-116 26 27     SPACE eurjchem-116 26 28 of of ADP eurjchem-116 26 29     SPACE eurjchem-116 26 30 voglibose voglibose NOUN eurjchem-116 26 31     SPACE eurjchem-116 26 32 was be AUX eurjchem-116 26 33     SPACE eurjchem-116 26 34 constructed construct VERB eurjchem-116 26 35     SPACE eurjchem-116 26 36 over over ADP eurjchem-116 26 37     SPACE eurjchem-116 26 38 a a DET eurjchem-116 26 39     SPACE eurjchem-116 26 40 concentration concentration NOUN eurjchem-116 26 41     SPACE eurjchem-116 26 42 range range NOUN eurjchem-116 26 43     SPACE eurjchem-116 26 44 of of ADP eurjchem-116 26 45     SPACE eurjchem-116 26 46 10‐100 10‐100 NUM eurjchem-116 26 47     SPACE eurjchem-116 26 48 µg µg VERB eurjchem-116 26 49 / / SYM eurjchem-116 26 50 ml ml NOUN eurjchem-116 26 51 . . PUNCT eurjchem-116 26 52     SPACE eurjchem-116 26 53 for for ADP eurjchem-116 26 54     SPACE eurjchem-116 26 55 each each DET eurjchem-116 26 56     SPACE eurjchem-116 26 57 standard standard NOUN eurjchem-116 26 58     SPACE eurjchem-116 26 59 curve curve NOUN eurjchem-116 26 60 , , PUNCT eurjchem-116 26 61     SPACE eurjchem-116 26 62 six six NUM eurjchem-116 26 63     SPACE eurjchem-116 26 64 different different ADJ eurjchem-116 26 65     SPACE eurjchem-116 26 66 concentrations concentration NOUN eurjchem-116 26 67     SPACE eurjchem-116 26 68 were be AUX eurjchem-116 26 69     SPACE eurjchem-116 26 70 used use VERB eurjchem-116 26 71 . . PUNCT eurjchem-116 26 72     SPACE eurjchem-116 27 1 the the DET eurjchem-116 27 2     SPACE eurjchem-116 27 3 calibration calibration NOUN eurjchem-116 27 4     SPACE eurjchem-116 27 5 plot plot NOUN eurjchem-116 27 6     SPACE eurjchem-116 27 7 was be AUX eurjchem-116 27 8     SPACE eurjchem-116 27 9 generated generate VERB eurjchem-116 27 10     SPACE eurjchem-116 27 11 by by ADP eurjchem-116 27 12     SPACE eurjchem-116 27 13 replicate replicate VERB eurjchem-116 27 14     SPACE eurjchem-116 27 15 analysis analysis NOUN eurjchem-116 27 16     SPACE eurjchem-116 27 17 ( ( PUNCT eurjchem-116 27 18 n n CCONJ eurjchem-116 27 19     SPACE eurjchem-116 27 20 = = NOUN eurjchem-116 27 21     SPACE eurjchem-116 27 22 6 6 NUM eurjchem-116 27 23 ) ) PUNCT eurjchem-116 27 24     SPACE eurjchem-116 27 25 at at ADP eurjchem-116 27 26     SPACE eurjchem-116 27 27 all all DET eurjchem-116 27 28     SPACE eurjchem-116 27 29 concentration concentration NOUN eurjchem-116 27 30     SPACE eurjchem-116 27 31 levels level NOUN eurjchem-116 27 32     SPACE eurjchem-116 27 33 and and CCONJ eurjchem-116 27 34     SPACE eurjchem-116 27 35 the the DET eurjchem-116 27 36     SPACE eurjchem-116 27 37 linear linear ADJ eurjchem-116 27 38     SPACE eurjchem-116 27 39 relationship relationship NOUN eurjchem-116 27 40     SPACE eurjchem-116 27 41 was be AUX eurjchem-116 27 42     SPACE eurjchem-116 27 43 evaluated evaluate VERB eurjchem-116 27 44     SPACE eurjchem-116 27 45 using use VERB eurjchem-116 27 46     SPACE eurjchem-116 27 47 the the DET eurjchem-116 27 48     SPACE eurjchem-116 27 49 least least ADJ eurjchem-116 27 50     SPACE eurjchem-116 27 51 square square ADJ eurjchem-116 27 52     SPACE eurjchem-116 27 53 method method NOUN eurjchem-116 27 54     SPACE eurjchem-116 27 55 within within ADP eurjchem-116 27 56     SPACE eurjchem-116 27 57 microsoft microsoft PROPN eurjchem-116 27 58     SPACE eurjchem-116 27 59 excel excel PROPN eurjchem-116 27 60 ® ® NOUN eurjchem-116 27 61     SPACE eurjchem-116 27 62 program program NOUN eurjchem-116 27 63 . . PUNCT eurjchem-116 27 64         SPACE eurjchem-116 28 1 2.5.2 2.5.2 NUM eurjchem-116 28 2 . . PUNCT eurjchem-116 28 3     SPACE eurjchem-116 28 4 precision precision NOUN eurjchem-116 28 5     SPACE eurjchem-116 28 6 and and CCONJ eurjchem-116 28 7     SPACE eurjchem-116 28 8 accuracy accuracy NOUN eurjchem-116 28 9         SPACE eurjchem-116 28 10 both both DET eurjchem-116 28 11     SPACE eurjchem-116 28 12 repeatability repeatability NOUN eurjchem-116 28 13     SPACE eurjchem-116 28 14 ( ( PUNCT eurjchem-116 28 15 within within ADP eurjchem-116 28 16     SPACE eurjchem-116 28 17 a a DET eurjchem-116 28 18     SPACE eurjchem-116 28 19 day day NOUN eurjchem-116 28 20     SPACE eurjchem-116 28 21 precision precision NOUN eurjchem-116 28 22 ) ) PUNCT eurjchem-116 28 23     SPACE eurjchem-116 28 24 and and CCONJ eurjchem-116 28 25     SPACE eurjchem-116 28 26 reproducibility reproducibility NOUN eurjchem-116 28 27     SPACE eurjchem-116 28 28 ( ( PUNCT eurjchem-116 28 29 between between ADP eurjchem-116 28 30     SPACE eurjchem-116 28 31 days day NOUN eurjchem-116 28 32     SPACE eurjchem-116 28 33 precision precision NOUN eurjchem-116 28 34 ) ) PUNCT eurjchem-116 28 35     SPACE eurjchem-116 28 36 were be AUX eurjchem-116 28 37     SPACE eurjchem-116 28 38 determined determine VERB eurjchem-116 28 39     SPACE eurjchem-116 28 40 as as SCONJ eurjchem-116 28 41     SPACE eurjchem-116 28 42 follows follow VERB eurjchem-116 28 43 . . PUNCT eurjchem-116 28 44     SPACE eurjchem-116 29 1 solutions solution NOUN eurjchem-116 29 2     SPACE eurjchem-116 29 3 containing contain VERB eurjchem-116 29 4     SPACE eurjchem-116 29 5 lowest low ADJ eurjchem-116 29 6 , , PUNCT eurjchem-116 29 7     SPACE eurjchem-116 29 8 intermediate intermediate ADJ eurjchem-116 29 9 , , PUNCT eurjchem-116 29 10     SPACE eurjchem-116 29 11 and and CCONJ eurjchem-116 29 12     SPACE eurjchem-116 29 13 highest high ADJ eurjchem-116 29 14     SPACE eurjchem-116 29 15 concentrations concentration NOUN eurjchem-116 29 16     SPACE eurjchem-116 29 17 of of ADP eurjchem-116 29 18     SPACE eurjchem-116 29 19 the the DET eurjchem-116 29 20     SPACE eurjchem-116 29 21 calibration calibration NOUN eurjchem-116 29 22     SPACE eurjchem-116 29 23 curve curve NOUN eurjchem-116 29 24 , , PUNCT eurjchem-116 29 25     SPACE eurjchem-116 29 26 i.e. i.e. X eurjchem-116 29 27     SPACE eurjchem-116 29 28 10 10 NUM eurjchem-116 29 29 , , PUNCT eurjchem-116 29 30     SPACE eurjchem-116 29 31 50 50 NUM eurjchem-116 29 32 , , PUNCT eurjchem-116 29 33     SPACE eurjchem-116 29 34 100 100 NUM eurjchem-116 29 35     SPACE eurjchem-116 29 36 µg µg VERB eurjchem-116 29 37 / / SYM eurjchem-116 29 38 ml ml VERB eurjchem-116 29 39     SPACE eurjchem-116 29 40 were be AUX eurjchem-116 29 41     SPACE eurjchem-116 29 42 prepared prepare VERB eurjchem-116 29 43 . . PUNCT eurjchem-116 29 44     SPACE eurjchem-116 29 45 six six NUM eurjchem-116 29 46     SPACE eurjchem-116 29 47 injections injection NOUN eurjchem-116 29 48     SPACE eurjchem-116 29 49 at at ADP eurjchem-116 29 50     SPACE eurjchem-116 29 51 each each PRON eurjchem-116 29 52     SPACE eurjchem-116 29 53 of of ADP eurjchem-116 29 54     SPACE eurjchem-116 29 55 the the DET eurjchem-116 29 56     SPACE eurjchem-116 29 57 specified specify VERB eurjchem-116 29 58     SPACE eurjchem-116 29 59 concentration concentration NOUN eurjchem-116 29 60     SPACE eurjchem-116 29 61 levels level NOUN eurjchem-116 29 62     SPACE eurjchem-116 29 63 were be AUX eurjchem-116 29 64     SPACE eurjchem-116 29 65 injected inject VERB eurjchem-116 29 66     SPACE eurjchem-116 29 67 within within ADP eurjchem-116 29 68     SPACE eurjchem-116 29 69 the the DET eurjchem-116 29 70     SPACE eurjchem-116 29 71 same same ADJ eurjchem-116 29 72     SPACE eurjchem-116 29 73 day day NOUN eurjchem-116 29 74     SPACE eurjchem-116 29 75 for for ADP eurjchem-116 29 76     SPACE eurjchem-116 29 77 repeatability repeatability NOUN eurjchem-116 29 78 , , PUNCT eurjchem-116 29 79     SPACE eurjchem-116 29 80 and and CCONJ eurjchem-116 29 81     SPACE eurjchem-116 29 82 over over ADP eurjchem-116 29 83     SPACE eurjchem-116 29 84 a a DET eurjchem-116 29 85     SPACE eurjchem-116 29 86 period period NOUN eurjchem-116 29 87     SPACE eurjchem-116 29 88 of of ADP eurjchem-116 29 89     SPACE eurjchem-116 29 90 3 3 NUM eurjchem-116 29 91     SPACE eurjchem-116 29 92 days day NOUN eurjchem-116 29 93     SPACE eurjchem-116 29 94 ( ( PUNCT eurjchem-116 29 95 6‐injections 6‐injection NOUN eurjchem-116 29 96 / / SYM eurjchem-116 29 97 day day NOUN eurjchem-116 29 98 ) ) PUNCT eurjchem-116 29 99     SPACE eurjchem-116 29 100 for for ADP eurjchem-116 29 101     SPACE eurjchem-116 29 102 reproducibility reproducibility NOUN eurjchem-116 29 103 . . PUNCT eurjchem-116 29 104     SPACE eurjchem-116 30 1 mean mean VERB eurjchem-116 30 2     SPACE eurjchem-116 30 3 and and CCONJ eurjchem-116 30 4     SPACE eurjchem-116 30 5 relative relative ADJ eurjchem-116 30 6     SPACE eurjchem-116 30 7 standard standard NOUN eurjchem-116 30 8     SPACE eurjchem-116 30 9 deviation deviation NOUN eurjchem-116 30 10     SPACE eurjchem-116 30 11 were be AUX eurjchem-116 30 12     SPACE eurjchem-116 30 13 calculated calculate VERB eurjchem-116 30 14     SPACE eurjchem-116 30 15 and and CCONJ eurjchem-116 30 16     SPACE eurjchem-116 30 17 used use VERB eurjchem-116 30 18     SPACE eurjchem-116 30 19 to to PART eurjchem-116 30 20     SPACE eurjchem-116 30 21 judge judge VERB eurjchem-116 30 22     SPACE eurjchem-116 30 23 accuracy accuracy NOUN eurjchem-116 30 24     SPACE eurjchem-116 30 25 and and CCONJ eurjchem-116 30 26     SPACE eurjchem-116 30 27 precision precision NOUN eurjchem-116 30 28     SPACE eurjchem-116 30 29 of of ADP eurjchem-116 30 30     SPACE eurjchem-116 30 31 the the DET eurjchem-116 30 32     SPACE eurjchem-116 30 33 method method NOUN eurjchem-116 30 34 . . PUNCT eurjchem-116 30 35     SPACE eurjchem-116 31 1 both both DET eurjchem-116 31 2     SPACE eurjchem-116 31 3 intra‐day intra‐day NOUN eurjchem-116 31 4     SPACE eurjchem-116 31 5 and and CCONJ eurjchem-116 31 6     SPACE eurjchem-116 31 7 inter‐day inter‐day NOUN eurjchem-116 31 8     SPACE eurjchem-116 31 9 samples sample NOUN eurjchem-116 31 10     SPACE eurjchem-116 31 11 were be AUX eurjchem-116 31 12     SPACE eurjchem-116 31 13 calibrated calibrate VERB eurjchem-116 31 14     SPACE eurjchem-116 31 15 with with SCONJ eurjchem-116 31 16     SPACE eurjchem-116 31 17 standard standard ADJ eurjchem-116 31 18     SPACE eurjchem-116 31 19 curves curve NOUN eurjchem-116 31 20     SPACE eurjchem-116 31 21 concurrently concurrently ADV eurjchem-116 31 22     SPACE eurjchem-116 31 23 prepared prepare VERB eurjchem-116 31 24     SPACE eurjchem-116 31 25 on on ADP eurjchem-116 31 26     SPACE eurjchem-116 31 27 the the DET eurjchem-116 31 28     SPACE eurjchem-116 31 29 day day NOUN eurjchem-116 31 30     SPACE eurjchem-116 31 31 of of ADP eurjchem-116 31 32     SPACE eurjchem-116 31 33 analysis analysis NOUN eurjchem-116 31 34 . . PUNCT eurjchem-116 31 35     SPACE eurjchem-116 32 1 accuracy accuracy NOUN eurjchem-116 32 2     SPACE eurjchem-116 32 3 was be AUX eurjchem-116 32 4     SPACE eurjchem-116 32 5 determined determine VERB eurjchem-116 32 6     SPACE eurjchem-116 32 7 as as ADP eurjchem-116 32 8     SPACE eurjchem-116 32 9 % % NOUN eurjchem-116 32 10 bias bias NOUN eurjchem-116 32 11     SPACE eurjchem-116 32 12 of of ADP eurjchem-116 32 13     SPACE eurjchem-116 32 14 vgb vgb ADJ eurjchem-116 32 15     SPACE eurjchem-116 32 16 amount amount NOUN eurjchem-116 32 17     SPACE eurjchem-116 32 18 found find VERB eurjchem-116 32 19 . . PUNCT eurjchem-116 32 20         SPACE eurjchem-116 33 1 2.5.3 2.5.3 NUM eurjchem-116 33 2 . . PUNCT eurjchem-116 33 3     SPACE eurjchem-116 33 4 limit limit NOUN eurjchem-116 33 5     SPACE eurjchem-116 33 6 of of ADP eurjchem-116 33 7     SPACE eurjchem-116 33 8 detection detection NOUN eurjchem-116 33 9     SPACE eurjchem-116 33 10 and and CCONJ eurjchem-116 33 11     SPACE eurjchem-116 33 12 limit limit NOUN eurjchem-116 33 13     SPACE eurjchem-116 33 14 of of ADP eurjchem-116 33 15     SPACE eurjchem-116 33 16 quantification quantification NOUN eurjchem-116 33 17         SPACE eurjchem-116 33 18 signal‐to‐noise signal‐to‐noise NOUN eurjchem-116 33 19     SPACE eurjchem-116 33 20 ratio ratio NOUN eurjchem-116 33 21     SPACE eurjchem-116 33 22 was be AUX eurjchem-116 33 23     SPACE eurjchem-116 33 24 used use VERB eurjchem-116 33 25     SPACE eurjchem-116 33 26 for for ADP eurjchem-116 33 27     SPACE eurjchem-116 33 28 the the DET eurjchem-116 33 29     SPACE eurjchem-116 33 30 estimation estimation NOUN eurjchem-116 33 31     SPACE eurjchem-116 33 32 of of ADP eurjchem-116 33 33     SPACE eurjchem-116 33 34 limit limit NOUN eurjchem-116 33 35     SPACE eurjchem-116 33 36 of of ADP eurjchem-116 33 37     SPACE eurjchem-116 33 38 detection detection NOUN eurjchem-116 33 39     SPACE eurjchem-116 33 40 and and CCONJ eurjchem-116 33 41     SPACE eurjchem-116 33 42 quantification quantification NOUN eurjchem-116 33 43 . . PUNCT eurjchem-116 33 44     SPACE eurjchem-116 34 1 the the DET eurjchem-116 34 2     SPACE eurjchem-116 34 3 limit limit NOUN eurjchem-116 34 4     SPACE eurjchem-116 34 5 of of ADP eurjchem-116 34 6     SPACE eurjchem-116 34 7 detection detection NOUN eurjchem-116 34 8     SPACE eurjchem-116 34 9 ( ( PUNCT eurjchem-116 34 10 lod lod PROPN eurjchem-116 34 11 ) ) PUNCT eurjchem-116 34 12     SPACE eurjchem-116 34 13 was be AUX eurjchem-116 34 14     SPACE eurjchem-116 34 15 defined define VERB eurjchem-116 34 16     SPACE eurjchem-116 34 17 as as ADP eurjchem-116 34 18     SPACE eurjchem-116 34 19 the the DET eurjchem-116 34 20     SPACE eurjchem-116 34 21 lowest low ADJ eurjchem-116 34 22     SPACE eurjchem-116 34 23 concentration concentration NOUN eurjchem-116 34 24     SPACE eurjchem-116 34 25 resulting result VERB eurjchem-116 34 26     SPACE eurjchem-116 34 27 in in ADP eurjchem-116 34 28     SPACE eurjchem-116 34 29 peak peak NOUN eurjchem-116 34 30     SPACE eurjchem-116 34 31 area area NOUN eurjchem-116 34 32     SPACE eurjchem-116 34 33 of of ADP eurjchem-116 34 34     SPACE eurjchem-116 34 35 three three NUM eurjchem-116 34 36     SPACE eurjchem-116 34 37 times time NOUN eurjchem-116 34 38     SPACE eurjchem-116 34 39 the the DET eurjchem-116 34 40     SPACE eurjchem-116 34 41 baseline baseline NOUN eurjchem-116 34 42     SPACE eurjchem-116 34 43 noise noise NOUN eurjchem-116 34 44 . . PUNCT eurjchem-116 34 45     SPACE eurjchem-116 35 1 the the DET eurjchem-116 35 2     SPACE eurjchem-116 35 3 limit limit NOUN eurjchem-116 35 4     SPACE eurjchem-116 35 5 if if SCONJ eurjchem-116 35 6     SPACE eurjchem-116 35 7 quantification quantification NOUN eurjchem-116 35 8     SPACE eurjchem-116 35 9 ( ( PUNCT eurjchem-116 35 10 loq loq PROPN eurjchem-116 35 11 ) ) PUNCT eurjchem-116 35 12     SPACE eurjchem-116 35 13 was be AUX eurjchem-116 35 14     SPACE eurjchem-116 35 15 defined define VERB eurjchem-116 35 16     SPACE eurjchem-116 35 17 as as ADP eurjchem-116 35 18     SPACE eurjchem-116 35 19 the the DET eurjchem-116 35 20     SPACE eurjchem-116 35 21 lowest low ADJ eurjchem-116 35 22     SPACE eurjchem-116 35 23 concentration concentration NOUN eurjchem-116 35 24     SPACE eurjchem-116 35 25 resulting result VERB eurjchem-116 35 26     SPACE eurjchem-116 35 27 in in ADP eurjchem-116 35 28     SPACE eurjchem-116 35 29 peak peak NOUN eurjchem-116 35 30     SPACE eurjchem-116 35 31 area area NOUN eurjchem-116 35 32     SPACE eurjchem-116 35 33 with with ADP eurjchem-116 35 34     SPACE eurjchem-116 35 35 signal‐to‐noise signal‐to‐noise NOUN eurjchem-116 35 36     SPACE eurjchem-116 35 37 ratio ratio NOUN eurjchem-116 35 38     SPACE eurjchem-116 35 39 higher high ADJ eurjchem-116 35 40     SPACE eurjchem-116 35 41 than than ADP eurjchem-116 35 42     SPACE eurjchem-116 35 43 10 10 NUM eurjchem-116 35 44     SPACE eurjchem-116 35 45 [ [ PUNCT eurjchem-116 35 46 11 11 NUM eurjchem-116 35 47 ] ] PUNCT eurjchem-116 35 48 , , PUNCT eurjchem-116 35 49     SPACE eurjchem-116 35 50 with with ADP eurjchem-116 35 51     SPACE eurjchem-116 35 52 precision precision NOUN eurjchem-116 35 53     SPACE eurjchem-116 35 54 ( ( PUNCT eurjchem-116 35 55 the the DET eurjchem-116 35 56     SPACE eurjchem-116 35 57 relative relative ADJ eurjchem-116 35 58     SPACE eurjchem-116 35 59 standard standard ADJ eurjchem-116 35 60     SPACE eurjchem-116 35 61 deviation deviation NOUN eurjchem-116 35 62 , , PUNCT eurjchem-116 35 63     SPACE eurjchem-116 35 64 % % NOUN eurjchem-116 35 65     SPACE eurjchem-116 35 66 r.s.d r.s.d NOUN eurjchem-116 35 67 . . PUNCT eurjchem-116 35 68 ) ) PUNCT eurjchem-116 35 69     SPACE eurjchem-116 35 70 and and CCONJ eurjchem-116 35 71     SPACE eurjchem-116 35 72 accuracy accuracy NOUN eurjchem-116 35 73     SPACE eurjchem-116 35 74 ( ( PUNCT eurjchem-116 35 75 % % NOUN eurjchem-116 35 76     SPACE eurjchem-116 35 77 bias bias NOUN eurjchem-116 35 78 ) ) PUNCT eurjchem-116 35 79     SPACE eurjchem-116 35 80 within within ADP eurjchem-116 35 81     SPACE eurjchem-116 35 82 ±10 ±10 NOUN eurjchem-116 35 83 % % NOUN eurjchem-116 35 84 . . PUNCT eurjchem-116 35 85         SPACE eurjchem-116 35 86 2.5.4 2.5.4 NUM eurjchem-116 35 87 . . PUNCT eurjchem-116 35 88     SPACE eurjchem-116 35 89 specificity specificity NOUN eurjchem-116 35 90     SPACE eurjchem-116 35 91 and and CCONJ eurjchem-116 35 92     SPACE eurjchem-116 35 93 selectivity selectivity NOUN eurjchem-116 35 94         SPACE eurjchem-116 35 95 the the DET eurjchem-116 35 96     SPACE eurjchem-116 35 97 specificity specificity NOUN eurjchem-116 35 98     SPACE eurjchem-116 35 99 of of ADP eurjchem-116 35 100     SPACE eurjchem-116 35 101 the the DET eurjchem-116 35 102     SPACE eurjchem-116 35 103 method method NOUN eurjchem-116 35 104     SPACE eurjchem-116 35 105 was be AUX eurjchem-116 35 106     SPACE eurjchem-116 35 107 established establish VERB eurjchem-116 35 108     SPACE eurjchem-116 35 109 through through ADP eurjchem-116 35 110     SPACE eurjchem-116 35 111 study study NOUN eurjchem-116 35 112     SPACE eurjchem-116 35 113 of of ADP eurjchem-116 35 114     SPACE eurjchem-116 35 115 resolution resolution NOUN eurjchem-116 35 116     SPACE eurjchem-116 35 117 factor factor NOUN eurjchem-116 35 118     SPACE eurjchem-116 35 119 of of ADP eurjchem-116 35 120     SPACE eurjchem-116 35 121 the the DET eurjchem-116 35 122     SPACE eurjchem-116 35 123 drug drug NOUN eurjchem-116 35 124     SPACE eurjchem-116 35 125 peak peak NOUN eurjchem-116 35 126     SPACE eurjchem-116 35 127 from from ADP eurjchem-116 35 128     SPACE eurjchem-116 35 129 the the DET eurjchem-116 35 130     SPACE eurjchem-116 35 131 nearest near ADJ eurjchem-116 35 132     SPACE eurjchem-116 35 133 resolving resolving NOUN eurjchem-116 35 134     SPACE eurjchem-116 35 135 peak peak NOUN eurjchem-116 35 136 , , PUNCT eurjchem-116 35 137     SPACE eurjchem-116 35 138 and and CCONJ eurjchem-116 35 139     SPACE eurjchem-116 35 140 also also ADV eurjchem-116 35 141     SPACE eurjchem-116 35 142 among among ADP eurjchem-116 35 143     SPACE eurjchem-116 35 144 all all DET eurjchem-116 35 145     SPACE eurjchem-116 35 146 other other ADJ eurjchem-116 35 147     SPACE eurjchem-116 35 148 peaks peak NOUN eurjchem-116 35 149 . . PUNCT eurjchem-116 35 150         SPACE eurjchem-116 36 1 2.5.5 2.5.5 NUM eurjchem-116 36 2 . . PUNCT eurjchem-116 36 3     SPACE eurjchem-116 36 4 stability stability NOUN eurjchem-116 36 5         SPACE eurjchem-116 36 6 drug drug NOUN eurjchem-116 36 7     SPACE eurjchem-116 36 8 solutions solution NOUN eurjchem-116 36 9     SPACE eurjchem-116 36 10 prepared prepare VERB eurjchem-116 36 11     SPACE eurjchem-116 36 12 with with ADP eurjchem-116 36 13     SPACE eurjchem-116 36 14 the the DET eurjchem-116 36 15     SPACE eurjchem-116 36 16 known know VERB eurjchem-116 36 17     SPACE eurjchem-116 36 18 amount amount NOUN eurjchem-116 36 19     SPACE eurjchem-116 36 20 of of ADP eurjchem-116 36 21     SPACE eurjchem-116 36 22 voglibose voglibose NOUN eurjchem-116 36 23     SPACE eurjchem-116 36 24 to to PART eurjchem-116 36 25     SPACE eurjchem-116 36 26 achieve achieve VERB eurjchem-116 36 27     SPACE eurjchem-116 36 28 the the DET eurjchem-116 36 29     SPACE eurjchem-116 36 30 concentration concentration NOUN eurjchem-116 36 31     SPACE eurjchem-116 36 32 of of ADP eurjchem-116 36 33     SPACE eurjchem-116 36 34 10 10 NUM eurjchem-116 36 35 , , PUNCT eurjchem-116 36 36     SPACE eurjchem-116 36 37 50 50 NUM eurjchem-116 36 38 , , PUNCT eurjchem-116 36 39     SPACE eurjchem-116 36 40 and and CCONJ eurjchem-116 36 41     SPACE eurjchem-116 36 42 100 100 NUM eurjchem-116 36 43     SPACE eurjchem-116 36 44 µg µg VERB eurjchem-116 36 45 / / SYM eurjchem-116 36 46 ml ml VERB eurjchem-116 36 47     SPACE eurjchem-116 36 48 ( ( PUNCT eurjchem-116 36 49 n n CCONJ eurjchem-116 36 50     SPACE eurjchem-116 36 51 = = NOUN eurjchem-116 36 52     SPACE eurjchem-116 36 53 3 3 NUM eurjchem-116 36 54 ) ) PUNCT eurjchem-116 36 55     SPACE eurjchem-116 36 56 and and CCONJ eurjchem-116 36 57     SPACE eurjchem-116 36 58 determined determine VERB eurjchem-116 36 59     SPACE eurjchem-116 36 60 for for ADP eurjchem-116 36 61     SPACE eurjchem-116 36 62 short‐term short‐term PROPN eurjchem-116 36 63     SPACE eurjchem-116 36 64 stability stability NOUN eurjchem-116 36 65     SPACE eurjchem-116 36 66 at at ADP eurjchem-116 36 67     SPACE eurjchem-116 36 68 room room NOUN eurjchem-116 36 69     SPACE eurjchem-116 36 70 temperature temperature NOUN eurjchem-116 36 71     SPACE eurjchem-116 36 72 for for ADP eurjchem-116 36 73     SPACE eurjchem-116 36 74 24 24 NUM eurjchem-116 36 75     SPACE eurjchem-116 36 76 h h NOUN eurjchem-116 36 77 , , PUNCT eurjchem-116 36 78     SPACE eurjchem-116 36 79 long‐term long‐term NOUN eurjchem-116 36 80     SPACE eurjchem-116 36 81 stability stability NOUN eurjchem-116 36 82     SPACE eurjchem-116 36 83 at at ADP eurjchem-116 36 84     SPACE eurjchem-116 36 85 ‐4 ‐4 PROPN eurjchem-116 36 86     SPACE eurjchem-116 36 87 oc oc NOUN eurjchem-116 36 88     SPACE eurjchem-116 36 89 and and CCONJ eurjchem-116 36 90     SPACE eurjchem-116 36 91 checked check VERB eurjchem-116 36 92     SPACE eurjchem-116 36 93 for for ADP eurjchem-116 36 94     SPACE eurjchem-116 36 95 up up ADP eurjchem-116 36 96     SPACE eurjchem-116 36 97 to to ADP eurjchem-116 36 98     SPACE eurjchem-116 36 99 1 1 NUM eurjchem-116 36 100     SPACE eurjchem-116 36 101 month month NOUN eurjchem-116 36 102     SPACE eurjchem-116 36 103 by by ADP eurjchem-116 36 104     SPACE eurjchem-116 36 105 comparing compare VERB eurjchem-116 36 106     SPACE eurjchem-116 36 107 the the DET eurjchem-116 36 108     SPACE eurjchem-116 36 109 results result NOUN eurjchem-116 36 110     SPACE eurjchem-116 36 111 with with ADP eurjchem-116 36 112     SPACE eurjchem-116 36 113 fresh fresh ADJ eurjchem-116 36 114     SPACE eurjchem-116 36 115 stock stock NOUN eurjchem-116 36 116     SPACE eurjchem-116 36 117 prepared prepare VERB eurjchem-116 36 118     SPACE eurjchem-116 36 119 on on ADP eurjchem-116 36 120     SPACE eurjchem-116 36 121 the the DET eurjchem-116 36 122     SPACE eurjchem-116 36 123 day day NOUN eurjchem-116 36 124     SPACE eurjchem-116 36 125 of of ADP eurjchem-116 36 126     SPACE eurjchem-116 36 127 analysis analysis NOUN eurjchem-116 36 128 . . PUNCT eurjchem-116 36 129     SPACE eurjchem-116 36 130 further far ADV eurjchem-116 36 131 , , PUNCT eurjchem-116 36 132     SPACE eurjchem-116 36 133 the the DET eurjchem-116 36 134     SPACE eurjchem-116 36 135 freeze freeze NOUN eurjchem-116 36 136 – – PUNCT eurjchem-116 36 137 thaw thaw NOUN eurjchem-116 36 138     SPACE eurjchem-116 36 139 ( ( PUNCT eurjchem-116 36 140 ‐20 ‐20 NOUN eurjchem-116 36 141     SPACE eurjchem-116 36 142 oc oc NOUN eurjchem-116 36 143 / / SYM eurjchem-116 36 144 room room NOUN eurjchem-116 36 145     SPACE eurjchem-116 36 146 temperature temperature NOUN eurjchem-116 36 147 ) ) PUNCT eurjchem-116 36 148     SPACE eurjchem-116 36 149 stability stability NOUN eurjchem-116 36 150     SPACE eurjchem-116 36 151 of of ADP eurjchem-116 36 152     SPACE eurjchem-116 36 153 the the DET eurjchem-116 36 154     SPACE eurjchem-116 36 155 voglibose voglibose NOUN eurjchem-116 36 156     SPACE eurjchem-116 36 157 samples sample NOUN eurjchem-116 36 158     SPACE eurjchem-116 36 159 were be AUX eurjchem-116 36 160     SPACE eurjchem-116 36 161 determined determine VERB eurjchem-116 36 162     SPACE eurjchem-116 36 163 for for ADP eurjchem-116 36 164     SPACE eurjchem-116 36 165 three three NUM eurjchem-116 36 166     SPACE eurjchem-116 36 167 cycles cycle NOUN eurjchem-116 36 168 . . PUNCT eurjchem-116 36 169     SPACE eurjchem-116 37 1 samples sample NOUN eurjchem-116 37 2     SPACE eurjchem-116 37 3 were be AUX eurjchem-116 37 4     SPACE eurjchem-116 37 5 considered consider VERB eurjchem-116 37 6     SPACE eurjchem-116 37 7 to to PART eurjchem-116 37 8     SPACE eurjchem-116 37 9 be be AUX eurjchem-116 37 10     SPACE eurjchem-116 37 11 stable stable ADJ eurjchem-116 37 12 , , PUNCT eurjchem-116 37 13     SPACE eurjchem-116 37 14 if if SCONJ eurjchem-116 37 15     SPACE eurjchem-116 37 16 the the DET eurjchem-116 37 17     SPACE eurjchem-116 37 18 assay assay NOUN eurjchem-116 37 19     SPACE eurjchem-116 37 20 values value NOUN eurjchem-116 37 21     SPACE eurjchem-116 37 22 were be AUX eurjchem-116 37 23     SPACE eurjchem-116 37 24 within within ADP eurjchem-116 37 25     SPACE eurjchem-116 37 26 the the DET eurjchem-116 37 27     SPACE eurjchem-116 37 28 acceptable acceptable ADJ eurjchem-116 37 29     SPACE eurjchem-116 37 30 limits limit NOUN eurjchem-116 37 31     SPACE eurjchem-116 37 32 of of ADP eurjchem-116 37 33     SPACE eurjchem-116 37 34 accuracy accuracy NOUN eurjchem-116 37 35     SPACE eurjchem-116 37 36 and and CCONJ eurjchem-116 37 37     SPACE eurjchem-116 37 38 precision precision NOUN eurjchem-116 37 39 . . PUNCT eurjchem-116 37 40         SPACE eurjchem-116 38 1 2.6 2.6 NUM eurjchem-116 38 2 . . PUNCT eurjchem-116 38 3     SPACE eurjchem-116 38 4 recovery recovery NOUN eurjchem-116 38 5     SPACE eurjchem-116 38 6 of of ADP eurjchem-116 38 7     SPACE eurjchem-116 38 8 voglibose voglibose NOUN eurjchem-116 38 9     SPACE eurjchem-116 38 10 from from ADP eurjchem-116 38 11     SPACE eurjchem-116 38 12 formulations formulation NOUN eurjchem-116 38 13         SPACE eurjchem-116 38 14 the the DET eurjchem-116 38 15     SPACE eurjchem-116 38 16 recovery recovery NOUN eurjchem-116 38 17     SPACE eurjchem-116 38 18 of of ADP eurjchem-116 38 19     SPACE eurjchem-116 38 20 an an DET eurjchem-116 38 21     SPACE eurjchem-116 38 22 analyte analyte NOUN eurjchem-116 38 23     SPACE eurjchem-116 38 24 is be AUX eurjchem-116 38 25     SPACE eurjchem-116 38 26 the the DET eurjchem-116 38 27     SPACE eurjchem-116 38 28 extraction extraction NOUN eurjchem-116 38 29     SPACE eurjchem-116 38 30 efficiency efficiency NOUN eurjchem-116 38 31     SPACE eurjchem-116 38 32 of of ADP eurjchem-116 38 33     SPACE eurjchem-116 38 34 an an DET eurjchem-116 38 35     SPACE eurjchem-116 38 36 analytical analytical ADJ eurjchem-116 38 37     SPACE eurjchem-116 38 38 process process NOUN eurjchem-116 38 39 , , PUNCT eurjchem-116 38 40     SPACE eurjchem-116 38 41 reported report VERB eurjchem-116 38 42     SPACE eurjchem-116 38 43 as as ADP eurjchem-116 38 44     SPACE eurjchem-116 38 45 a a DET eurjchem-116 38 46     SPACE eurjchem-116 38 47 percentage percentage NOUN eurjchem-116 38 48     SPACE eurjchem-116 38 49 of of ADP eurjchem-116 38 50     SPACE eurjchem-116 38 51 the the DET eurjchem-116 38 52     SPACE eurjchem-116 38 53 known know VERB eurjchem-116 38 54     SPACE eurjchem-116 38 55 amount amount NOUN eurjchem-116 38 56     SPACE eurjchem-116 38 57 of of ADP eurjchem-116 38 58     SPACE eurjchem-116 38 59 an an DET eurjchem-116 38 60     SPACE eurjchem-116 38 61 analyte analyte NOUN eurjchem-116 38 62     SPACE eurjchem-116 38 63 carried carry VERB eurjchem-116 38 64     SPACE eurjchem-116 38 65 through through ADP eurjchem-116 38 66     SPACE eurjchem-116 38 67 the the DET eurjchem-116 38 68     SPACE eurjchem-116 38 69 sample sample NOUN eurjchem-116 38 70     SPACE eurjchem-116 38 71 extraction extraction NOUN eurjchem-116 38 72     SPACE eurjchem-116 38 73 and and CCONJ eurjchem-116 38 74     SPACE eurjchem-116 38 75 processing processing NOUN eurjchem-116 38 76     SPACE eurjchem-116 38 77 steps step NOUN eurjchem-116 38 78     SPACE eurjchem-116 38 79 of of ADP eurjchem-116 38 80     SPACE eurjchem-116 38 81 the the DET eurjchem-116 38 82     SPACE eurjchem-116 38 83 method method NOUN eurjchem-116 38 84 . . PUNCT eurjchem-116 38 85     SPACE eurjchem-116 38 86 mobile mobile ADJ eurjchem-116 38 87     SPACE eurjchem-116 38 88 phase phase NOUN eurjchem-116 38 89     SPACE eurjchem-116 38 90 was be AUX eurjchem-116 38 91     SPACE eurjchem-116 38 92 most most ADJ eurjchem-116 38 93     SPACE eurjchem-116 38 94 efficient efficient ADJ eurjchem-116 38 95     SPACE eurjchem-116 38 96 in in ADP eurjchem-116 38 97     SPACE eurjchem-116 38 98 extracting extract VERB eurjchem-116 38 99     SPACE eurjchem-116 38 100 vgb vgb NOUN eurjchem-116 38 101     SPACE eurjchem-116 38 102 from from ADP eurjchem-116 38 103     SPACE eurjchem-116 38 104 formulation formulation NOUN eurjchem-116 38 105     SPACE eurjchem-116 38 106 and and CCONJ eurjchem-116 38 107     SPACE eurjchem-116 38 108 had have VERB eurjchem-116 38 109     SPACE eurjchem-116 38 110 a a DET eurjchem-116 38 111     SPACE eurjchem-116 38 112 small small ADJ eurjchem-116 38 113     SPACE eurjchem-116 38 114 variation variation NOUN eurjchem-116 38 115     SPACE eurjchem-116 38 116 in in ADP eurjchem-116 38 117     SPACE eurjchem-116 38 118 extraction extraction NOUN eurjchem-116 38 119     SPACE eurjchem-116 38 120 recoveries recovery NOUN eurjchem-116 38 121     SPACE eurjchem-116 38 122 over over ADP eurjchem-116 38 123     SPACE eurjchem-116 38 124 the the DET eurjchem-116 38 125     SPACE eurjchem-116 38 126 concentration concentration NOUN eurjchem-116 38 127     SPACE eurjchem-116 38 128 range range NOUN eurjchem-116 38 129 . . PUNCT eurjchem-116 38 130     SPACE eurjchem-116 39 1 samples sample NOUN eurjchem-116 39 2     SPACE eurjchem-116 39 3 were be AUX eurjchem-116 39 4     SPACE eurjchem-116 39 5 prepared prepare VERB eurjchem-116 39 6     SPACE eurjchem-116 39 7 in in ADP eurjchem-116 39 8     SPACE eurjchem-116 39 9 triplicate triplicate VERB eurjchem-116 39 10     SPACE eurjchem-116 39 11 at at ADP eurjchem-116 39 12     SPACE eurjchem-116 39 13 three three NUM eurjchem-116 39 14     SPACE eurjchem-116 39 15 concentrations concentration NOUN eurjchem-116 39 16     SPACE eurjchem-116 39 17 10 10 NUM eurjchem-116 39 18 , , PUNCT eurjchem-116 39 19     SPACE eurjchem-116 39 20 50 50 NUM eurjchem-116 39 21 , , PUNCT eurjchem-116 39 22     SPACE eurjchem-116 39 23 and and CCONJ eurjchem-116 39 24     SPACE eurjchem-116 39 25 100 100 NUM eurjchem-116 39 26     SPACE eurjchem-116 39 27 µg µg VERB eurjchem-116 39 28 / / SYM eurjchem-116 39 29 ml ml NOUN eurjchem-116 39 30     SPACE eurjchem-116 39 31 of of ADP eurjchem-116 39 32     SPACE eurjchem-116 39 33 vgb vgb NOUN eurjchem-116 39 34     SPACE eurjchem-116 39 35 and and CCONJ eurjchem-116 39 36     SPACE eurjchem-116 39 37 assayed assayed ADJ eurjchem-116 39 38     SPACE eurjchem-116 39 39 as as SCONJ eurjchem-116 39 40     SPACE eurjchem-116 39 41 described describe VERB eurjchem-116 39 42     SPACE eurjchem-116 39 43 above above ADV eurjchem-116 39 44 . . PUNCT eurjchem-116 39 45     SPACE eurjchem-116 40 1 the the DET eurjchem-116 40 2     SPACE eurjchem-116 40 3 extraction extraction NOUN eurjchem-116 40 4     SPACE eurjchem-116 40 5 efficiency efficiency NOUN eurjchem-116 40 6     SPACE eurjchem-116 40 7 of of ADP eurjchem-116 40 8     SPACE eurjchem-116 40 9 voglibose voglibose NOUN eurjchem-116 40 10     SPACE eurjchem-116 40 11 was be AUX eurjchem-116 40 12     SPACE eurjchem-116 40 13 determined determine VERB eurjchem-116 40 14     SPACE eurjchem-116 40 15 by by ADP eurjchem-116 40 16     SPACE eurjchem-116 40 17 compa‐ compa‐ PROPN eurjchem-116 40 18 ring ring NOUN eurjchem-116 40 19     SPACE eurjchem-116 40 20 the the DET eurjchem-116 40 21     SPACE eurjchem-116 40 22 peak peak NOUN eurjchem-116 40 23     SPACE eurjchem-116 40 24 areas area NOUN eurjchem-116 40 25     SPACE eurjchem-116 40 26 measured measure VERB eurjchem-116 40 27     SPACE eurjchem-116 40 28 after after ADP eurjchem-116 40 29     SPACE eurjchem-116 40 30 analysis analysis NOUN eurjchem-116 40 31     SPACE eurjchem-116 40 32 of of ADP eurjchem-116 40 33     SPACE eurjchem-116 40 34 samples sample NOUN eurjchem-116 40 35     SPACE eurjchem-116 40 36 from from ADP eurjchem-116 40 37     SPACE eurjchem-116 40 38 formulation formulation NOUN eurjchem-116 40 39     SPACE eurjchem-116 40 40 with with ADP eurjchem-116 40 41     SPACE eurjchem-116 40 42 those those PRON eurjchem-116 40 43     SPACE eurjchem-116 40 44 found find VERB eurjchem-116 40 45     SPACE eurjchem-116 40 46 after after ADP eurjchem-116 40 47     SPACE eurjchem-116 40 48 direct direct ADJ eurjchem-116 40 49     SPACE eurjchem-116 40 50 injection injection NOUN eurjchem-116 40 51     SPACE eurjchem-116 40 52 of of ADP eurjchem-116 40 53     SPACE eurjchem-116 40 54 unextracted unextracte VERB eurjchem-116 40 55     SPACE eurjchem-116 40 56 ( ( PUNCT eurjchem-116 40 57 pure pure ADJ eurjchem-116 40 58 ) ) PUNCT eurjchem-116 40 59     SPACE eurjchem-116 40 60 samples sample NOUN eurjchem-116 40 61     SPACE eurjchem-116 40 62 into into ADP eurjchem-116 40 63     SPACE eurjchem-116 40 64 the the DET eurjchem-116 40 65     SPACE eurjchem-116 40 66 chromatographic chromatographic ADJ eurjchem-116 40 67     SPACE eurjchem-116 40 68 system system NOUN eurjchem-116 40 69     SPACE eurjchem-116 40 70 at at ADP eurjchem-116 40 71     SPACE eurjchem-116 40 72 the the DET eurjchem-116 40 73     SPACE eurjchem-116 40 74 same same ADJ eurjchem-116 40 75     SPACE eurjchem-116 40 76 concentration concentration NOUN eurjchem-116 40 77     SPACE eurjchem-116 40 78 levels level NOUN eurjchem-116 40 79 . . PUNCT eurjchem-116 40 80         SPACE eurjchem-116 41 1 3 3 NUM eurjchem-116 41 2 . . PUNCT eurjchem-116 41 3     SPACE eurjchem-116 41 4 results result VERB eurjchem-116 41 5     SPACE eurjchem-116 41 6 and and CCONJ eurjchem-116 41 7     SPACE eurjchem-116 41 8 discussion discussion NOUN eurjchem-116 41 9         SPACE eurjchem-116 41 10 3.1 3.1 NUM eurjchem-116 41 11 . . PUNCT eurjchem-116 41 12     SPACE eurjchem-116 41 13 optimization optimization NOUN eurjchem-116 41 14     SPACE eurjchem-116 41 15 of of ADP eurjchem-116 41 16     SPACE eurjchem-116 41 17 chromatographic chromatographic ADJ eurjchem-116 41 18     SPACE eurjchem-116 41 19 method method NOUN eurjchem-116 41 20         SPACE eurjchem-116 41 21 figure figure NOUN eurjchem-116 41 22     SPACE eurjchem-116 41 23 2a 2a NUM eurjchem-116 41 24     SPACE eurjchem-116 41 25 shows show VERB eurjchem-116 41 26     SPACE eurjchem-116 41 27 an an DET eurjchem-116 41 28     SPACE eurjchem-116 41 29 lc lc NOUN eurjchem-116 41 30     SPACE eurjchem-116 41 31 elution elution NOUN eurjchem-116 41 32     SPACE eurjchem-116 41 33 of of ADP eurjchem-116 41 34     SPACE eurjchem-116 41 35 voglibose voglibose NOUN eurjchem-116 41 36 . . PUNCT eurjchem-116 41 37     SPACE eurjchem-116 41 38 during during ADP eurjchem-116 41 39     SPACE eurjchem-116 41 40 the the DET eurjchem-116 41 41     SPACE eurjchem-116 41 42 development development NOUN eurjchem-116 41 43     SPACE eurjchem-116 41 44 phase phase NOUN eurjchem-116 41 45 , , PUNCT eurjchem-116 41 46     SPACE eurjchem-116 41 47 the the DET eurjchem-116 41 48     SPACE eurjchem-116 41 49 mobile mobile ADJ eurjchem-116 41 50     SPACE eurjchem-116 41 51 phase phase NOUN eurjchem-116 41 52     SPACE eurjchem-116 41 53 containing contain VERB eurjchem-116 41 54     SPACE eurjchem-116 41 55 methanol‐ methanol‐ NOUN eurjchem-116 41 56 water water NOUN eurjchem-116 41 57     SPACE eurjchem-116 41 58 resulted result VERB eurjchem-116 41 59     SPACE eurjchem-116 41 60 in in ADP eurjchem-116 41 61     SPACE eurjchem-116 41 62 broad broad ADJ eurjchem-116 41 63     SPACE eurjchem-116 41 64 and and CCONJ eurjchem-116 41 65     SPACE eurjchem-116 41 66 asymmetric asymmetric ADJ eurjchem-116 41 67     SPACE eurjchem-116 41 68 peak peak NOUN eurjchem-116 41 69     SPACE eurjchem-116 41 70 with with ADP eurjchem-116 41 71     SPACE eurjchem-116 41 72 a a DET eurjchem-116 41 73     SPACE eurjchem-116 41 74 greater great ADJ eurjchem-116 41 75     SPACE eurjchem-116 41 76 tailing tail VERB eurjchem-116 41 77     SPACE eurjchem-116 41 78 factor factor NOUN eurjchem-116 41 79     SPACE eurjchem-116 41 80 ( ( PUNCT eurjchem-116 41 81 > > NOUN eurjchem-116 41 82 2 2 NUM eurjchem-116 41 83 ) ) PUNCT eurjchem-116 41 84 . . PUNCT eurjchem-116 41 85     SPACE eurjchem-116 42 1 the the DET eurjchem-116 42 2     SPACE eurjchem-116 42 3 successful successful ADJ eurjchem-116 42 4     SPACE eurjchem-116 42 5 use use NOUN eurjchem-116 42 6     SPACE eurjchem-116 42 7 of of ADP eurjchem-116 42 8     SPACE eurjchem-116 42 9 acetonitrile acetonitrile NOUN eurjchem-116 42 10     SPACE eurjchem-116 42 11 and and CCONJ eurjchem-116 42 12     SPACE eurjchem-116 42 13 water water NOUN eurjchem-116 42 14     SPACE eurjchem-116 42 15 resulted result VERB eurjchem-116 42 16     SPACE eurjchem-116 42 17 in in ADP eurjchem-116 42 18     SPACE eurjchem-116 42 19 drastic drastic ADJ eurjchem-116 42 20     SPACE eurjchem-116 42 21 reduction reduction NOUN eurjchem-116 42 22     SPACE eurjchem-116 42 23 of of ADP eurjchem-116 42 24     SPACE eurjchem-116 42 25 peak peak NOUN eurjchem-116 42 26     SPACE eurjchem-116 42 27 tailing tailing NOUN eurjchem-116 42 28 , , PUNCT eurjchem-116 42 29     SPACE eurjchem-116 42 30 which which PRON eurjchem-116 42 31     SPACE eurjchem-116 42 32 was be AUX eurjchem-116 42 33     SPACE eurjchem-116 42 34 found find VERB eurjchem-116 42 35     SPACE eurjchem-116 42 36 to to PART eurjchem-116 42 37     SPACE eurjchem-116 42 38 be be AUX eurjchem-116 42 39     SPACE eurjchem-116 42 40 within within ADP eurjchem-116 42 41     SPACE eurjchem-116 42 42 the the DET eurjchem-116 42 43     SPACE eurjchem-116 42 44 acceptable acceptable ADJ eurjchem-116 42 45     SPACE eurjchem-116 42 46 limit limit NOUN eurjchem-116 42 47     SPACE eurjchem-116 42 48 ( ( PUNCT eurjchem-116 42 49 1.5 1.5 NUM eurjchem-116 42 50 ) ) PUNCT eurjchem-116 42 51     SPACE eurjchem-116 42 52 resulting result VERB eurjchem-116 42 53     SPACE eurjchem-116 42 54 good good ADJ eurjchem-116 42 55     SPACE eurjchem-116 42 56 peak peak NOUN eurjchem-116 42 57     SPACE eurjchem-116 42 58 symmetry symmetry NOUN eurjchem-116 42 59     SPACE eurjchem-116 42 60 and and CCONJ eurjchem-116 42 61     SPACE eurjchem-116 42 62 resolution resolution NOUN eurjchem-116 42 63 . . PUNCT eurjchem-116 42 64     SPACE eurjchem-116 43 1 the the DET eurjchem-116 43 2     SPACE eurjchem-116 43 3 mobile mobile ADJ eurjchem-116 43 4     SPACE eurjchem-116 43 5 phase phase NOUN eurjchem-116 43 6     SPACE eurjchem-116 43 7 optimized optimize VERB eurjchem-116 43 8     SPACE eurjchem-116 43 9 contained contain VERB eurjchem-116 43 10     SPACE eurjchem-116 43 11 water water NOUN eurjchem-116 43 12     SPACE eurjchem-116 43 13 and and CCONJ eurjchem-116 43 14     SPACE eurjchem-116 43 15 acetonitrile acetonitrile NOUN eurjchem-116 43 16     SPACE eurjchem-116 43 17 ( ( PUNCT eurjchem-116 43 18 50 50 NUM eurjchem-116 43 19 : : PUNCT eurjchem-116 43 20     SPACE eurjchem-116 43 21 50 50 NUM eurjchem-116 43 22 ) ) PUNCT eurjchem-116 43 23     SPACE eurjchem-116 43 24 at at ADP eurjchem-116 43 25     SPACE eurjchem-116 43 26 0.5 0.5 NUM eurjchem-116 43 27     SPACE eurjchem-116 43 28 ml ml NOUN eurjchem-116 43 29 / / SYM eurjchem-116 43 30 min min NOUN eurjchem-116 43 31     SPACE eurjchem-116 43 32 flow flow NOUN eurjchem-116 43 33     SPACE eurjchem-116 43 34 rate rate NOUN eurjchem-116 43 35 . . PUNCT eurjchem-116 43 36     SPACE eurjchem-116 44 1 the the DET eurjchem-116 44 2     SPACE eurjchem-116 44 3 retention retention NOUN eurjchem-116 44 4     SPACE eurjchem-116 44 5 time time NOUN eurjchem-116 44 6     SPACE eurjchem-116 44 7 was be AUX eurjchem-116 44 8     SPACE eurjchem-116 44 9 found find VERB eurjchem-116 44 10     SPACE eurjchem-116 44 11 to to PART eurjchem-116 44 12     SPACE eurjchem-116 44 13 be be AUX eurjchem-116 44 14     SPACE eurjchem-116 44 15 3.264 3.264 NUM eurjchem-116 44 16     SPACE eurjchem-116 44 17 min min NOUN eurjchem-116 44 18     SPACE eurjchem-116 44 19 for for ADP eurjchem-116 44 20     SPACE eurjchem-116 44 21 vgb vgb NOUN eurjchem-116 44 22 . . PUNCT eurjchem-116 44 23     SPACE eurjchem-116 45 1 there there PRON eurjchem-116 45 2     SPACE eurjchem-116 45 3 were be AUX eurjchem-116 45 4     SPACE eurjchem-116 45 5 no no DET eurjchem-116 45 6     SPACE eurjchem-116 45 7 interferences interference NOUN eurjchem-116 45 8     SPACE eurjchem-116 45 9 at at ADP eurjchem-116 45 10     SPACE eurjchem-116 45 11 drug drug NOUN eurjchem-116 45 12     SPACE eurjchem-116 45 13 retention retention NOUN eurjchem-116 45 14     SPACE eurjchem-116 45 15 time time NOUN eurjchem-116 45 16 . . PUNCT eurjchem-116 45 17         SPACE eurjchem-116 45 18 figure figure NOUN eurjchem-116 45 19     SPACE eurjchem-116 45 20 2 2 NUM eurjchem-116 45 21 . . PUNCT eurjchem-116 45 22     SPACE eurjchem-116 45 23 chromatogram chromatogram PROPN eurjchem-116 45 24     SPACE eurjchem-116 45 25 showing show VERB eurjchem-116 45 26     SPACE eurjchem-116 45 27 ( ( PUNCT eurjchem-116 45 28 a a X eurjchem-116 45 29 ) ) PUNCT eurjchem-116 45 30     SPACE eurjchem-116 45 31 voglibose voglibose NOUN eurjchem-116 45 32     SPACE eurjchem-116 45 33 ( ( PUNCT eurjchem-116 45 34 80 80 NUM eurjchem-116 45 35     SPACE eurjchem-116 45 36 µg µg NOUN eurjchem-116 45 37 / / SYM eurjchem-116 45 38 ml ml NOUN eurjchem-116 45 39 ) ) PUNCT eurjchem-116 45 40     SPACE eurjchem-116 45 41 in in ADP eurjchem-116 45 42     SPACE eurjchem-116 45 43 pure pure ADJ eurjchem-116 45 44     SPACE eurjchem-116 45 45 form form NOUN eurjchem-116 45 46     SPACE eurjchem-116 45 47 ( ( PUNCT eurjchem-116 45 48 b b NOUN eurjchem-116 45 49 ) ) PUNCT eurjchem-116 45 50     SPACE eurjchem-116 45 51 voglibose voglibose NOUN eurjchem-116 45 52     SPACE eurjchem-116 45 53 ( ( PUNCT eurjchem-116 45 54 30 30 NUM eurjchem-116 45 55     SPACE eurjchem-116 45 56 µg µg NOUN eurjchem-116 45 57 / / SYM eurjchem-116 45 58 ml ml NOUN eurjchem-116 45 59 ) ) PUNCT eurjchem-116 45 60     SPACE eurjchem-116 45 61 in in ADP eurjchem-116 45 62     SPACE eurjchem-116 45 63 formulations formulation NOUN eurjchem-116 45 64 ) ) PUNCT eurjchem-116 45 65     SPACE eurjchem-116 45 66 and and CCONJ eurjchem-116 45 67     SPACE eurjchem-116 45 68 ( ( PUNCT eurjchem-116 45 69 c c NOUN eurjchem-116 45 70 ) ) PUNCT eurjchem-116 45 71     SPACE eurjchem-116 45 72 blank blank NOUN eurjchem-116 45 73     SPACE eurjchem-116 45 74 run run NOUN eurjchem-116 45 75     SPACE eurjchem-116 45 76 devoid devoid ADJ eurjchem-116 45 77     SPACE eurjchem-116 45 78 of of ADP eurjchem-116 45 79     SPACE eurjchem-116 45 80 sample sample NOUN eurjchem-116 45 81 . . PUNCT eurjchem-116 45 82         SPACE eurjchem-116 46 1 voglibose voglibose NOUN eurjchem-116 46 2     SPACE eurjchem-116 46 3 was be AUX eurjchem-116 46 4     SPACE eurjchem-116 46 5 determined determine VERB eurjchem-116 46 6     SPACE eurjchem-116 46 7 using use VERB eurjchem-116 46 8     SPACE eurjchem-116 46 9 high high ADJ eurjchem-116 46 10     SPACE eurjchem-116 46 11 performance performance NOUN eurjchem-116 46 12     SPACE eurjchem-116 46 13 liquid liquid NOUN eurjchem-116 46 14     SPACE eurjchem-116 46 15 chromatography chromatography NOUN eurjchem-116 46 16     SPACE eurjchem-116 46 17 with with ADP eurjchem-116 46 18     SPACE eurjchem-116 46 19 refractive refractive ADJ eurjchem-116 46 20     SPACE eurjchem-116 46 21 index index NOUN eurjchem-116 46 22     SPACE eurjchem-116 46 23 detector detector NOUN eurjchem-116 46 24     SPACE eurjchem-116 46 25 and and CCONJ eurjchem-116 46 26     SPACE eurjchem-116 46 27 found find VERB eurjchem-116 46 28     SPACE eurjchem-116 46 29 to to PART eurjchem-116 46 30     SPACE eurjchem-116 46 31 be be AUX eurjchem-116 46 32     SPACE eurjchem-116 46 33 well well ADV eurjchem-116 46 34     SPACE eurjchem-116 46 35 suited suited ADJ eurjchem-116 46 36     SPACE eurjchem-116 46 37 technique technique NOUN eurjchem-116 46 38     SPACE eurjchem-116 46 39 for for ADP eurjchem-116 46 40     SPACE eurjchem-116 46 41 the the DET eurjchem-116 46 42     SPACE eurjchem-116 46 43 analysis analysis NOUN eurjchem-116 46 44     SPACE eurjchem-116 46 45 of of ADP eurjchem-116 46 46     SPACE eurjchem-116 46 47 non‐uv non‐uv PROPN eurjchem-116 46 48     SPACE eurjchem-116 46 49 absorbing absorbing ADJ eurjchem-116 46 50     SPACE eurjchem-116 46 51 compound compound NOUN eurjchem-116 46 52     SPACE eurjchem-116 46 53 without without ADP eurjchem-116 46 54     SPACE eurjchem-116 46 55 derivatization derivatization NOUN eurjchem-116 46 56 . . PUNCT eurjchem-116 46 57     SPACE eurjchem-116 47 1 ri ri PROPN eurjchem-116 47 2     SPACE eurjchem-116 47 3 indicator indicator NOUN eurjchem-116 47 4     SPACE eurjchem-116 47 5 increased increase VERB eurjchem-116 47 6     SPACE eurjchem-116 47 7 the the DET eurjchem-116 47 8     SPACE eurjchem-116 47 9 sensitivity sensitivity NOUN eurjchem-116 47 10     SPACE eurjchem-116 47 11 of of ADP eurjchem-116 47 12     SPACE eurjchem-116 47 13 detection detection NOUN eurjchem-116 47 14 . . PUNCT eurjchem-116 47 15         SPACE eurjchem-116 47 16 264 264 NUM eurjchem-116 47 17     SPACE eurjchem-116 47 18 lakshmi lakshmi NOUN eurjchem-116 47 19     SPACE eurjchem-116 47 20 and and CCONJ eurjchem-116 47 21     SPACE eurjchem-116 47 22 rajesh rajesh PROPN eurjchem-116 47 23     SPACE eurjchem-116 47 24 / / SYM eurjchem-116 47 25     SPACE eurjchem-116 47 26 european european ADJ eurjchem-116 47 27     SPACE eurjchem-116 47 28 journal journal NOUN eurjchem-116 47 29     SPACE eurjchem-116 47 30 of of ADP eurjchem-116 47 31     SPACE eurjchem-116 47 32 chemistry chemistry NOUN eurjchem-116 47 33     SPACE eurjchem-116 47 34 1 1 NUM eurjchem-116 47 35     SPACE eurjchem-116 47 36 ( ( PUNCT eurjchem-116 47 37 4 4 NUM eurjchem-116 47 38 ) ) PUNCT eurjchem-116 47 39     SPACE eurjchem-116 47 40 ( ( PUNCT eurjchem-116 47 41 2010 2010 NUM eurjchem-116 47 42 ) ) PUNCT eurjchem-116 47 43     SPACE eurjchem-116 47 44 262­265 262­265 NOUN eurjchem-116 47 45         SPACE eurjchem-116 47 46 3.2 3.2 NUM eurjchem-116 47 47 . . PUNCT eurjchem-116 47 48     SPACE eurjchem-116 47 49 validation validation NOUN eurjchem-116 47 50     SPACE eurjchem-116 47 51 of of ADP eurjchem-116 47 52     SPACE eurjchem-116 47 53 the the DET eurjchem-116 47 54     SPACE eurjchem-116 47 55 proposed propose VERB eurjchem-116 47 56     SPACE eurjchem-116 47 57 method method NOUN eurjchem-116 47 58         SPACE eurjchem-116 47 59 3.2.1 3.2.1 NUM eurjchem-116 47 60 . . PUNCT eurjchem-116 47 61     SPACE eurjchem-116 47 62 linearity linearity NOUN eurjchem-116 47 63     SPACE eurjchem-116 47 64 and and CCONJ eurjchem-116 47 65     SPACE eurjchem-116 47 66 calibration calibration NOUN eurjchem-116 47 67     SPACE eurjchem-116 47 68 curve curve NOUN eurjchem-116 47 69           SPACE eurjchem-116 47 70 calibration calibration NOUN eurjchem-116 47 71     SPACE eurjchem-116 47 72 curve curve NOUN eurjchem-116 47 73     SPACE eurjchem-116 47 74 ( ( PUNCT eurjchem-116 47 75 peak peak NOUN eurjchem-116 47 76     SPACE eurjchem-116 47 77 area area NOUN eurjchem-116 47 78 ) ) PUNCT eurjchem-116 47 79     SPACE eurjchem-116 47 80 was be AUX eurjchem-116 47 81     SPACE eurjchem-116 47 82 constructed construct VERB eurjchem-116 47 83     SPACE eurjchem-116 47 84 by by ADP eurjchem-116 47 85     SPACE eurjchem-116 47 86 spiking spike VERB eurjchem-116 47 87     SPACE eurjchem-116 47 88 six six NUM eurjchem-116 47 89     SPACE eurjchem-116 47 90 different different ADJ eurjchem-116 47 91     SPACE eurjchem-116 47 92 concentrations concentration NOUN eurjchem-116 47 93     SPACE eurjchem-116 47 94 of of ADP eurjchem-116 47 95     SPACE eurjchem-116 47 96 vgb vgb ADJ eurjchem-116 47 97 . . PUNCT eurjchem-116 47 98     SPACE eurjchem-116 47 99 the the DET eurjchem-116 47 100     SPACE eurjchem-116 47 101 chromatographic chromatographic ADJ eurjchem-116 47 102     SPACE eurjchem-116 47 103 responses response NOUN eurjchem-116 47 104     SPACE eurjchem-116 47 105 were be AUX eurjchem-116 47 106     SPACE eurjchem-116 47 107 found find VERB eurjchem-116 47 108     SPACE eurjchem-116 47 109 to to PART eurjchem-116 47 110     SPACE eurjchem-116 47 111 be be AUX eurjchem-116 47 112     SPACE eurjchem-116 47 113 linear linear ADJ eurjchem-116 47 114     SPACE eurjchem-116 47 115 over over ADP eurjchem-116 47 116     SPACE eurjchem-116 47 117 an an DET eurjchem-116 47 118     SPACE eurjchem-116 47 119 analytical analytical ADJ eurjchem-116 47 120     SPACE eurjchem-116 47 121 range range NOUN eurjchem-116 47 122     SPACE eurjchem-116 47 123 of of ADP eurjchem-116 47 124     SPACE eurjchem-116 47 125 10‐100 10‐100 NUM eurjchem-116 47 126     SPACE eurjchem-116 47 127 µg µg VERB eurjchem-116 47 128 / / SYM eurjchem-116 47 129 ml ml VERB eurjchem-116 47 130     SPACE eurjchem-116 47 131 and and CCONJ eurjchem-116 47 132     SPACE eurjchem-116 47 133 found find VERB eurjchem-116 47 134     SPACE eurjchem-116 47 135 to to PART eurjchem-116 47 136     SPACE eurjchem-116 47 137 be be AUX eurjchem-116 47 138     SPACE eurjchem-116 47 139 quite quite ADV eurjchem-116 47 140     SPACE eurjchem-116 47 141 satisfactory satisfactory ADJ eurjchem-116 47 142     SPACE eurjchem-116 47 143 and and CCONJ eurjchem-116 47 144     SPACE eurjchem-116 47 145 reproducible reproducible VERB eurjchem-116 47 146     SPACE eurjchem-116 47 147 with with ADP eurjchem-116 47 148     SPACE eurjchem-116 47 149 time time NOUN eurjchem-116 47 150 . . PUNCT eurjchem-116 47 151     SPACE eurjchem-116 48 1 the the DET eurjchem-116 48 2     SPACE eurjchem-116 48 3 linear linear NOUN eurjchem-116 48 4     SPACE eurjchem-116 48 5 regression regression NOUN eurjchem-116 48 6     SPACE eurjchem-116 48 7 equation equation NOUN eurjchem-116 48 8     SPACE eurjchem-116 48 9 was be AUX eurjchem-116 48 10     SPACE eurjchem-116 48 11 calculated calculate VERB eurjchem-116 48 12     SPACE eurjchem-116 48 13 by by ADP eurjchem-116 48 14     SPACE eurjchem-116 48 15 the the DET eurjchem-116 48 16     SPACE eurjchem-116 48 17 least least ADJ eurjchem-116 48 18     SPACE eurjchem-116 48 19 squares square NOUN eurjchem-116 48 20     SPACE eurjchem-116 48 21 method method NOUN eurjchem-116 48 22     SPACE eurjchem-116 48 23 using use VERB eurjchem-116 48 24     SPACE eurjchem-116 48 25 microsoft microsoft PROPN eurjchem-116 48 26     SPACE eurjchem-116 48 27 excel excel PROPN eurjchem-116 48 28 ® ® NOUN eurjchem-116 48 29     SPACE eurjchem-116 48 30 program program NOUN eurjchem-116 48 31 . . PUNCT eurjchem-116 48 32     SPACE eurjchem-116 49 1 the the DET eurjchem-116 49 2     SPACE eurjchem-116 49 3 correlation correlation NOUN eurjchem-116 49 4     SPACE eurjchem-116 49 5 coefficient coefficient NOUN eurjchem-116 49 6     SPACE eurjchem-116 49 7 equals equal VERB eurjchem-116 49 8     SPACE eurjchem-116 49 9 0.9994 0.9994 NUM eurjchem-116 49 10 , , PUNCT eurjchem-116 49 11     SPACE eurjchem-116 49 12 indicating indicate VERB eurjchem-116 49 13     SPACE eurjchem-116 49 14 a a DET eurjchem-116 49 15     SPACE eurjchem-116 49 16 strong strong ADJ eurjchem-116 49 17     SPACE eurjchem-116 49 18 linear linear ADJ eurjchem-116 49 19     SPACE eurjchem-116 49 20 relationship relationship NOUN eurjchem-116 49 21     SPACE eurjchem-116 49 22 between between ADP eurjchem-116 49 23     SPACE eurjchem-116 49 24 the the DET eurjchem-116 49 25     SPACE eurjchem-116 49 26 variables variable NOUN eurjchem-116 49 27 . . PUNCT eurjchem-116 49 28     SPACE eurjchem-116 50 1 the the DET eurjchem-116 50 2     SPACE eurjchem-116 50 3 variance variance NOUN eurjchem-116 50 4     SPACE eurjchem-116 50 5 of of ADP eurjchem-116 50 6     SPACE eurjchem-116 50 7 response response NOUN eurjchem-116 50 8     SPACE eurjchem-116 50 9 variable variable NOUN eurjchem-116 50 10     SPACE eurjchem-116 50 11 s2yx s2yx NOUN eurjchem-116 50 12     SPACE eurjchem-116 50 13 calculated calculate VERB eurjchem-116 50 14     SPACE eurjchem-116 50 15 was be AUX eurjchem-116 50 16     SPACE eurjchem-116 50 17 1.86 1.86 NUM eurjchem-116 50 18 , , PUNCT eurjchem-116 50 19     SPACE eurjchem-116 50 20 indicates indicate VERB eurjchem-116 50 21     SPACE eurjchem-116 50 22 low low ADJ eurjchem-116 50 23     SPACE eurjchem-116 50 24 variability variability NOUN eurjchem-116 50 25     SPACE eurjchem-116 50 26 between between ADP eurjchem-116 50 27     SPACE eurjchem-116 50 28 the the DET eurjchem-116 50 29     SPACE eurjchem-116 50 30 estimated estimate VERB eurjchem-116 50 31     SPACE eurjchem-116 50 32 and and CCONJ eurjchem-116 50 33     SPACE eurjchem-116 50 34 calculated calculate VERB eurjchem-116 50 35     SPACE eurjchem-116 50 36 values value NOUN eurjchem-116 50 37 . . PUNCT eurjchem-116 50 38     SPACE eurjchem-116 51 1 this this PRON eurjchem-116 51 2     SPACE eurjchem-116 51 3 further far ADV eurjchem-116 51 4     SPACE eurjchem-116 51 5 confirms confirm VERB eurjchem-116 51 6     SPACE eurjchem-116 51 7 negligible negligible ADJ eurjchem-116 51 8     SPACE eurjchem-116 51 9 scattering scattering NOUN eurjchem-116 51 10     SPACE eurjchem-116 51 11 of of ADP eurjchem-116 51 12     SPACE eurjchem-116 51 13 the the DET eurjchem-116 51 14     SPACE eurjchem-116 51 15 experimental experimental ADJ eurjchem-116 51 16     SPACE eurjchem-116 51 17 data datum NOUN eurjchem-116 51 18     SPACE eurjchem-116 51 19 points point NOUN eurjchem-116 51 20     SPACE eurjchem-116 51 21 around around ADP eurjchem-116 51 22     SPACE eurjchem-116 51 23 the the DET eurjchem-116 51 24     SPACE eurjchem-116 51 25 line line NOUN eurjchem-116 51 26     SPACE eurjchem-116 51 27 of of ADP eurjchem-116 51 28     SPACE eurjchem-116 51 29 regression regression NOUN eurjchem-116 51 30     SPACE eurjchem-116 51 31 and and CCONJ eurjchem-116 51 32     SPACE eurjchem-116 51 33 good good ADJ eurjchem-116 51 34     SPACE eurjchem-116 51 35 sensitivity sensitivity NOUN eurjchem-116 51 36     SPACE eurjchem-116 51 37 of of ADP eurjchem-116 51 38     SPACE eurjchem-116 51 39 the the DET eurjchem-116 51 40     SPACE eurjchem-116 51 41 proposed propose VERB eurjchem-116 51 42     SPACE eurjchem-116 51 43 method method NOUN eurjchem-116 51 44 . . PUNCT eurjchem-116 51 45         SPACE eurjchem-116 52 1 3.2.2 3.2.2 NUM eurjchem-116 52 2 . . PUNCT eurjchem-116 52 3     SPACE eurjchem-116 52 4 precision precision NOUN eurjchem-116 52 5     SPACE eurjchem-116 52 6 and and CCONJ eurjchem-116 52 7     SPACE eurjchem-116 52 8 accuracy accuracy NOUN eurjchem-116 52 9         SPACE eurjchem-116 52 10 inter‐day inter‐day NOUN eurjchem-116 52 11     SPACE eurjchem-116 52 12 as as ADV eurjchem-116 52 13     SPACE eurjchem-116 52 14 well well ADV eurjchem-116 52 15     SPACE eurjchem-116 52 16 as as ADP eurjchem-116 52 17     SPACE eurjchem-116 52 18 intra‐day intra‐day NOUN eurjchem-116 52 19     SPACE eurjchem-116 52 20 replicates replicate NOUN eurjchem-116 52 21     SPACE eurjchem-116 52 22 of of ADP eurjchem-116 52 23     SPACE eurjchem-116 52 24 vgb vgb ADJ eurjchem-116 52 25 , , PUNCT eurjchem-116 52 26     SPACE eurjchem-116 52 27 gave give VERB eurjchem-116 52 28     SPACE eurjchem-116 52 29 an an DET eurjchem-116 52 30     SPACE eurjchem-116 52 31 r.s.d r.s.d NOUN eurjchem-116 52 32 . . PUNCT eurjchem-116 52 33     SPACE eurjchem-116 53 1 below below ADP eurjchem-116 53 2     SPACE eurjchem-116 53 3 2.12 2.12 NUM eurjchem-116 53 4     SPACE eurjchem-116 53 5 revealed reveal VERB eurjchem-116 53 6     SPACE eurjchem-116 53 7 that that SCONJ eurjchem-116 53 8     SPACE eurjchem-116 53 9 the the DET eurjchem-116 53 10     SPACE eurjchem-116 53 11 proposed propose VERB eurjchem-116 53 12     SPACE eurjchem-116 53 13 method method NOUN eurjchem-116 53 14     SPACE eurjchem-116 53 15 is be AUX eurjchem-116 53 16     SPACE eurjchem-116 53 17 highly highly ADV eurjchem-116 53 18     SPACE eurjchem-116 53 19 precise precise ADJ eurjchem-116 53 20 . . PUNCT eurjchem-116 53 21     SPACE eurjchem-116 53 22 accuracy accuracy NOUN eurjchem-116 53 23     SPACE eurjchem-116 53 24 data datum NOUN eurjchem-116 53 25     SPACE eurjchem-116 53 26 ( ( PUNCT eurjchem-116 53 27 % % INTJ eurjchem-116 53 28 bias bias NOUN eurjchem-116 53 29 ) ) PUNCT eurjchem-116 53 30     SPACE eurjchem-116 53 31 in in ADP eurjchem-116 53 32     SPACE eurjchem-116 53 33 the the DET eurjchem-116 53 34     SPACE eurjchem-116 53 35 present present ADJ eurjchem-116 53 36     SPACE eurjchem-116 53 37 study study NOUN eurjchem-116 53 38     SPACE eurjchem-116 53 39 ranged range VERB eurjchem-116 53 40     SPACE eurjchem-116 53 41 from from ADP eurjchem-116 53 42     SPACE eurjchem-116 53 43 ‐1.86 ‐1.86 NOUN eurjchem-116 53 44     SPACE eurjchem-116 53 45 to to ADP eurjchem-116 53 46     SPACE eurjchem-116 53 47 +0.11 +0.11 NOUN eurjchem-116 53 48     SPACE eurjchem-116 53 49 and and CCONJ eurjchem-116 53 50     SPACE eurjchem-116 53 51 indicated indicate VERB eurjchem-116 53 52     SPACE eurjchem-116 53 53 no no DET eurjchem-116 53 54     SPACE eurjchem-116 53 55 interference interference NOUN eurjchem-116 53 56     SPACE eurjchem-116 53 57 from from ADP eurjchem-116 53 58     SPACE eurjchem-116 53 59 formulation formulation NOUN eurjchem-116 53 60     SPACE eurjchem-116 53 61 excipients excipient NOUN eurjchem-116 53 62 . . PUNCT eurjchem-116 53 63     SPACE eurjchem-116 54 1 accuracy accuracy NOUN eurjchem-116 54 2     SPACE eurjchem-116 54 3 and and CCONJ eurjchem-116 54 4     SPACE eurjchem-116 54 5 precision precision NOUN eurjchem-116 54 6     SPACE eurjchem-116 54 7 calculated calculate VERB eurjchem-116 54 8     SPACE eurjchem-116 54 9 during during ADP eurjchem-116 54 10     SPACE eurjchem-116 54 11 the the DET eurjchem-116 54 12     SPACE eurjchem-116 54 13 intra‐ intra‐ NOUN eurjchem-116 54 14     SPACE eurjchem-116 54 15 and and CCONJ eurjchem-116 54 16     SPACE eurjchem-116 54 17 inter‐day inter‐day NOUN eurjchem-116 54 18     SPACE eurjchem-116 54 19 run run NOUN eurjchem-116 54 20     SPACE eurjchem-116 54 21 are be AUX eurjchem-116 54 22     SPACE eurjchem-116 54 23 given give VERB eurjchem-116 54 24     SPACE eurjchem-116 54 25 in in ADP eurjchem-116 54 26     SPACE eurjchem-116 54 27 table table NOUN eurjchem-116 54 28     SPACE eurjchem-116 54 29 1 1 NUM eurjchem-116 54 30 . . PUNCT eurjchem-116 54 31         SPACE eurjchem-116 54 32 table table NOUN eurjchem-116 54 33     SPACE eurjchem-116 54 34 1 1 NUM eurjchem-116 54 35 . . PUNCT eurjchem-116 54 36     SPACE eurjchem-116 54 37 precision precision NOUN eurjchem-116 54 38     SPACE eurjchem-116 54 39 and and CCONJ eurjchem-116 54 40     SPACE eurjchem-116 54 41 accuracy accuracy NOUN eurjchem-116 54 42     SPACE eurjchem-116 54 43 data datum NOUN eurjchem-116 54 44     SPACE eurjchem-116 54 45 for for ADP eurjchem-116 54 46     SPACE eurjchem-116 54 47 voglibose voglibose NOUN eurjchem-116 54 48     SPACE eurjchem-116 54 49 obtained obtain VERB eurjchem-116 54 50     SPACE eurjchem-116 54 51 by by ADP eurjchem-116 54 52     SPACE eurjchem-116 54 53 the the DET eurjchem-116 54 54     SPACE eurjchem-116 54 55 developed developed ADJ eurjchem-116 54 56     SPACE eurjchem-116 54 57 method method NOUN eurjchem-116 54 58 * * NOUN eurjchem-116 54 59 . . PUNCT eurjchem-116 54 60     SPACE eurjchem-116 54 61 day day NOUN eurjchem-116 54 62     SPACE eurjchem-116 54 63 precision precision NOUN eurjchem-116 54 64     SPACE eurjchem-116 54 65 and and CCONJ eurjchem-116 54 66     SPACE eurjchem-116 54 67 accuracy accuracy NOUN eurjchem-116 54 68     SPACE eurjchem-116 54 69 data data NOUN eurjchem-116 54 70     SPACE eurjchem-116 54 71 nominal nominal ADJ eurjchem-116 54 72     SPACE eurjchem-116 54 73 concentrations concentration NOUN eurjchem-116 54 74     SPACE eurjchem-116 54 75 ( ( PUNCT eurjchem-116 54 76 µg µg NOUN eurjchem-116 54 77 / / SYM eurjchem-116 54 78 ml ml NOUN eurjchem-116 54 79 ) ) PUNCT eurjchem-116 54 80     SPACE eurjchem-116 54 81 10 10 NUM eurjchem-116 54 82     SPACE eurjchem-116 54 83 50 50 NUM eurjchem-116 54 84     SPACE eurjchem-116 54 85 100 100 NUM eurjchem-116 54 86     SPACE eurjchem-116 54 87 day day NOUN eurjchem-116 54 88     SPACE eurjchem-116 54 89 1 1 NUM eurjchem-116 54 90     SPACE eurjchem-116 54 91 mean mean VERB eurjchem-116 54 92                             SPACE eurjchem-116 54 93 9.92 9.92 NUM eurjchem-116 54 94 50.02 50.02 NUM eurjchem-116 54 95     SPACE eurjchem-116 54 96 99.25 99.25 NUM eurjchem-116 54 97 s.d s.d PROPN eurjchem-116 54 98 . . PROPN eurjchem-116 54 99                             SPACE eurjchem-116 54 100 0.14 0.14 NUM eurjchem-116 54 101 1.01 1.01 NUM eurjchem-116 54 102     SPACE eurjchem-116 54 103 2.11 2.11 NUM eurjchem-116 54 104 % % NOUN eurjchem-116 54 105     SPACE eurjchem-116 54 106 r.s.d r.s.d NOUN eurjchem-116 54 107                   SPACE eurjchem-116 54 108 1.41 1.41 NUM eurjchem-116 54 109 2.02 2.02 NUM eurjchem-116 54 110     SPACE eurjchem-116 54 111 2.12 2.12 NUM eurjchem-116 54 112 % % NOUN eurjchem-116 54 113     SPACE eurjchem-116 54 114 bias bias NOUN eurjchem-116 54 115                       SPACE eurjchem-116 54 116 ‐0.8 ‐0.8 PROPN eurjchem-116 54 117 +0.04 +0.04 PROPN eurjchem-116 54 118     SPACE eurjchem-116 54 119 ‐0.75 ‐0.75 ADJ eurjchem-116 54 120 day day NOUN eurjchem-116 54 121     SPACE eurjchem-116 54 122 2 2 NUM eurjchem-116 54 123     SPACE eurjchem-116 54 124 mean mean VERB eurjchem-116 54 125                             SPACE eurjchem-116 54 126 9.89 9.89 NUM eurjchem-116 54 127 49.41 49.41 NUM eurjchem-116 54 128     SPACE eurjchem-116 54 129 100.11 100.11 NUM eurjchem-116 54 130 s.d s.d PROPN eurjchem-116 54 131 . . PROPN eurjchem-116 54 132                               SPACE eurjchem-116 54 133 0.13 0.13 NUM eurjchem-116 54 134 1.04 1.04 NUM eurjchem-116 54 135     SPACE eurjchem-116 54 136 1.97 1.97 NUM eurjchem-116 54 137 % % NOUN eurjchem-116 54 138     SPACE eurjchem-116 54 139 r.s.d r.s.d NOUN eurjchem-116 54 140                   SPACE eurjchem-116 54 141 1.31 1.31 NUM eurjchem-116 54 142 2.10 2.10 NUM eurjchem-116 54 143     SPACE eurjchem-116 54 144 1.96 1.96 NUM eurjchem-116 54 145 % % NOUN eurjchem-116 54 146     SPACE eurjchem-116 54 147 bias bias NOUN eurjchem-116 54 148                         SPACE eurjchem-116 54 149 ‐1.1 ‐1.1 ADJ eurjchem-116 54 150 ‐1.18 ‐1.18 PROPN eurjchem-116 54 151     SPACE eurjchem-116 54 152 +0.11 +0.11 PROPN eurjchem-116 54 153 day day NOUN eurjchem-116 54 154     SPACE eurjchem-116 54 155 3 3 NUM eurjchem-116 54 156     SPACE eurjchem-116 54 157 mean mean VERB eurjchem-116 54 158                             SPACE eurjchem-116 54 159 9.86 9.86 NUM eurjchem-116 54 160 49.07 49.07 NUM eurjchem-116 54 161     SPACE eurjchem-116 54 162 99.11 99.11 NUM eurjchem-116 54 163 s.d s.d PROPN eurjchem-116 54 164 . . PROPN eurjchem-116 54 165                               SPACE eurjchem-116 54 166 0.14 0.14 NUM eurjchem-116 54 167 1.04 1.04 NUM eurjchem-116 54 168     SPACE eurjchem-116 54 169 2.07 2.07 NUM eurjchem-116 54 170 % % NOUN eurjchem-116 54 171     SPACE eurjchem-116 54 172 r.s.d r.s.d VERB eurjchem-116 54 173                     SPACE eurjchem-116 54 174 1.42 1.42 NUM eurjchem-116 54 175 2.12 2.12 NUM eurjchem-116 54 176     SPACE eurjchem-116 54 177 2.09 2.09 NUM eurjchem-116 54 178 % % NOUN eurjchem-116 54 179     SPACE eurjchem-116 54 180 bias bias NOUN eurjchem-116 54 181                           SPACE eurjchem-116 54 182 ‐1.4 ‐1.4 NOUN eurjchem-116 54 183 ‐1.86 ‐1.86 NUM eurjchem-116 54 184     SPACE eurjchem-116 54 185 ‐0.89 ‐0.89 NOUN eurjchem-116 54 186 * * PUNCT eurjchem-116 54 187     SPACE eurjchem-116 54 188 each each DET eurjchem-116 54 189     SPACE eurjchem-116 54 190 mean mean ADJ eurjchem-116 54 191     SPACE eurjchem-116 54 192 value value NOUN eurjchem-116 54 193     SPACE eurjchem-116 54 194 is be AUX eurjchem-116 54 195     SPACE eurjchem-116 54 196 the the DET eurjchem-116 54 197     SPACE eurjchem-116 54 198 result result NOUN eurjchem-116 54 199     SPACE eurjchem-116 54 200 of of ADP eurjchem-116 54 201     SPACE eurjchem-116 54 202 triplicate triplicate VERB eurjchem-116 54 203     SPACE eurjchem-116 54 204 analysis analysis NOUN eurjchem-116 54 205 ; ; PUNCT eurjchem-116 54 206       SPACE eurjchem-116 54 207 % % NOUN eurjchem-116 54 208     SPACE eurjchem-116 54 209 r.s.d r.s.d NOUN eurjchem-116 54 210     SPACE eurjchem-116 54 211 = = NOUN eurjchem-116 54 212     SPACE eurjchem-116 54 213 ( ( PUNCT eurjchem-116 54 214 s.d./mean s.d./mean ADJ eurjchem-116 54 215 ) ) PUNCT eurjchem-116 54 216     SPACE eurjchem-116 54 217 x x NOUN eurjchem-116 54 218     SPACE eurjchem-116 54 219 100 100 NUM eurjchem-116 54 220 , , PUNCT eurjchem-116 54 221       SPACE eurjchem-116 54 222 % % NOUN eurjchem-116 54 223     SPACE eurjchem-116 54 224 bias bias NOUN eurjchem-116 54 225     SPACE eurjchem-116 54 226 = = NOUN eurjchem-116 54 227     SPACE eurjchem-116 55 1 [ [ X eurjchem-116 55 2 ( ( PUNCT eurjchem-116 55 3 measured measure VERB eurjchem-116 55 4     SPACE eurjchem-116 55 5 value‐true value‐true NOUN eurjchem-116 55 6     SPACE eurjchem-116 55 7 value)/true value)/true ADJ eurjchem-116 55 8     SPACE eurjchem-116 55 9 value value NOUN eurjchem-116 55 10 ] ] PUNCT eurjchem-116 55 11     SPACE eurjchem-116 55 12 x x NOUN eurjchem-116 55 13     SPACE eurjchem-116 55 14 100 100 NUM eurjchem-116 55 15 . . PUNCT eurjchem-116 55 16         SPACE eurjchem-116 56 1 3.2.3 3.2.3 NUM eurjchem-116 56 2 . . PUNCT eurjchem-116 56 3     SPACE eurjchem-116 56 4 lod lod PROPN eurjchem-116 56 5     SPACE eurjchem-116 56 6 and and CCONJ eurjchem-116 56 7     SPACE eurjchem-116 56 8 loq loq PROPN eurjchem-116 56 9         SPACE eurjchem-116 56 10 the the DET eurjchem-116 56 11     SPACE eurjchem-116 56 12 lod lod PROPN eurjchem-116 56 13     SPACE eurjchem-116 56 14 and and CCONJ eurjchem-116 56 15     SPACE eurjchem-116 56 16 loq loq PROPN eurjchem-116 56 17     SPACE eurjchem-116 56 18 were be AUX eurjchem-116 56 19     SPACE eurjchem-116 56 20 found find VERB eurjchem-116 56 21     SPACE eurjchem-116 56 22 to to PART eurjchem-116 56 23     SPACE eurjchem-116 56 24 be be AUX eurjchem-116 56 25     SPACE eurjchem-116 56 26 2.91 2.91 NUM eurjchem-116 56 27     SPACE eurjchem-116 56 28 and and CCONJ eurjchem-116 56 29     SPACE eurjchem-116 56 30 9.70 9.70 NUM eurjchem-116 56 31     SPACE eurjchem-116 56 32 µg µg NOUN eurjchem-116 56 33 / / SYM eurjchem-116 56 34 ml ml NOUN eurjchem-116 56 35 , , PUNCT eurjchem-116 56 36     SPACE eurjchem-116 56 37 respectively respectively ADV eurjchem-116 56 38 . . PUNCT eurjchem-116 56 39     SPACE eurjchem-116 56 40 when when SCONJ eurjchem-116 56 41     SPACE eurjchem-116 56 42 this this DET eurjchem-116 56 43     SPACE eurjchem-116 56 44 method method NOUN eurjchem-116 56 45     SPACE eurjchem-116 56 46 is be AUX eurjchem-116 56 47     SPACE eurjchem-116 56 48 applied apply VERB eurjchem-116 56 49     SPACE eurjchem-116 56 50 to to PART eurjchem-116 56 51     SPACE eurjchem-116 56 52 formulation formulation NOUN eurjchem-116 56 53     SPACE eurjchem-116 56 54 samples sample NOUN eurjchem-116 56 55 , , PUNCT eurjchem-116 56 56     SPACE eurjchem-116 56 57 its its PRON eurjchem-116 56 58     SPACE eurjchem-116 56 59 sensitivity sensitivity NOUN eurjchem-116 56 60     SPACE eurjchem-116 56 61 was be AUX eurjchem-116 56 62     SPACE eurjchem-116 56 63 found find VERB eurjchem-116 56 64     SPACE eurjchem-116 56 65 to to PART eurjchem-116 56 66     SPACE eurjchem-116 56 67 be be AUX eurjchem-116 56 68     SPACE eurjchem-116 56 69 adequate adequate ADJ eurjchem-116 56 70     SPACE eurjchem-116 56 71 for for ADP eurjchem-116 56 72     SPACE eurjchem-116 56 73 assay assay NOUN eurjchem-116 56 74     SPACE eurjchem-116 56 75 of of ADP eurjchem-116 56 76     SPACE eurjchem-116 56 77 the the DET eurjchem-116 56 78     SPACE eurjchem-116 56 79 formulations formulation NOUN eurjchem-116 56 80 . . PUNCT eurjchem-116 56 81         SPACE eurjchem-116 57 1 3.2.4 3.2.4 NUM eurjchem-116 57 2 . . PUNCT eurjchem-116 57 3     SPACE eurjchem-116 57 4 specificity specificity NOUN eurjchem-116 57 5     SPACE eurjchem-116 57 6 and and CCONJ eurjchem-116 57 7     SPACE eurjchem-116 57 8 selectivity selectivity NOUN eurjchem-116 57 9         SPACE eurjchem-116 57 10 any any DET eurjchem-116 57 11     SPACE eurjchem-116 57 12 potential potential ADJ eurjchem-116 57 13     SPACE eurjchem-116 57 14 interference interference NOUN eurjchem-116 57 15     SPACE eurjchem-116 57 16 ( ( PUNCT eurjchem-116 57 17 overlapping overlap VERB eurjchem-116 57 18     SPACE eurjchem-116 57 19 peaks peak NOUN eurjchem-116 57 20 ) ) PUNCT eurjchem-116 57 21     SPACE eurjchem-116 57 22 due due ADJ eurjchem-116 57 23     SPACE eurjchem-116 57 24 to to PART eurjchem-116 57 25     SPACE eurjchem-116 57 26 formulation formulation NOUN eurjchem-116 57 27     SPACE eurjchem-116 57 28 excipients excipient NOUN eurjchem-116 57 29     SPACE eurjchem-116 57 30 were be AUX eurjchem-116 57 31     SPACE eurjchem-116 57 32 within within ADP eurjchem-116 57 33     SPACE eurjchem-116 57 34 2min 2min NOUN eurjchem-116 57 35     SPACE eurjchem-116 57 36 only only ADV eurjchem-116 57 37     SPACE eurjchem-116 57 38 ( ( PUNCT eurjchem-116 57 39 figure figure NOUN eurjchem-116 57 40     SPACE eurjchem-116 57 41 2b 2b NOUN eurjchem-116 57 42 ) ) PUNCT eurjchem-116 57 43 , , PUNCT eurjchem-116 57 44     SPACE eurjchem-116 57 45 later later ADV eurjchem-116 57 46     SPACE eurjchem-116 57 47 on on SCONJ eurjchem-116 57 48     SPACE eurjchem-116 57 49 there there PRON eurjchem-116 57 50     SPACE eurjchem-116 57 51 was be AUX eurjchem-116 57 52     SPACE eurjchem-116 57 53 no no DET eurjchem-116 57 54     SPACE eurjchem-116 57 55 significant significant ADJ eurjchem-116 57 56     SPACE eurjchem-116 57 57 interference interference NOUN eurjchem-116 57 58     SPACE eurjchem-116 57 59 from from ADP eurjchem-116 57 60     SPACE eurjchem-116 57 61 blank blank NOUN eurjchem-116 57 62     SPACE eurjchem-116 57 63 ( ( PUNCT eurjchem-116 57 64 figure figure NOUN eurjchem-116 57 65     SPACE eurjchem-116 57 66 2c 2c NUM eurjchem-116 57 67 ) ) PUNCT eurjchem-116 57 68     SPACE eurjchem-116 57 69 that that PRON eurjchem-116 57 70     SPACE eurjchem-116 57 71 affected affect VERB eurjchem-116 57 72     SPACE eurjchem-116 57 73 the the DET eurjchem-116 57 74     SPACE eurjchem-116 57 75 response response NOUN eurjchem-116 57 76     SPACE eurjchem-116 57 77 of of ADP eurjchem-116 57 78     SPACE eurjchem-116 57 79 voglibose voglibose NOUN eurjchem-116 57 80 . . PUNCT eurjchem-116 57 81         SPACE eurjchem-116 58 1 3.2.5 3.2.5 NUM eurjchem-116 58 2 . . PUNCT eurjchem-116 58 3     SPACE eurjchem-116 58 4 stability stability NOUN eurjchem-116 58 5         SPACE eurjchem-116 58 6 the the DET eurjchem-116 58 7     SPACE eurjchem-116 58 8 study study NOUN eurjchem-116 58 9     SPACE eurjchem-116 58 10 indicated indicate VERB eurjchem-116 58 11     SPACE eurjchem-116 58 12 that that SCONJ eurjchem-116 58 13     SPACE eurjchem-116 58 14 samples sample NOUN eurjchem-116 58 15     SPACE eurjchem-116 58 16 were be AUX eurjchem-116 58 17     SPACE eurjchem-116 58 18 stable stable ADJ eurjchem-116 58 19     SPACE eurjchem-116 58 20 for for ADP eurjchem-116 58 21     SPACE eurjchem-116 58 22 24 24 NUM eurjchem-116 58 23     SPACE eurjchem-116 58 24 h h NOUN eurjchem-116 58 25     SPACE eurjchem-116 58 26 ( ( PUNCT eurjchem-116 58 27 short‐term short‐term PROPN eurjchem-116 58 28 ) ) PUNCT eurjchem-116 58 29     SPACE eurjchem-116 58 30 at at ADP eurjchem-116 58 31     SPACE eurjchem-116 58 32 room room NOUN eurjchem-116 58 33     SPACE eurjchem-116 58 34 temperature temperature NOUN eurjchem-116 58 35     SPACE eurjchem-116 58 36 and and CCONJ eurjchem-116 58 37     SPACE eurjchem-116 58 38 samples sample NOUN eurjchem-116 58 39     SPACE eurjchem-116 58 40 stored store VERB eurjchem-116 58 41     SPACE eurjchem-116 58 42 at at ADP eurjchem-116 58 43     SPACE eurjchem-116 58 44 ‐4 ‐4 PROPN eurjchem-116 58 45     SPACE eurjchem-116 58 46 oc oc NOUN eurjchem-116 58 47 , , PUNCT eurjchem-116 58 48     SPACE eurjchem-116 58 49 were be AUX eurjchem-116 58 50     SPACE eurjchem-116 58 51 injected inject VERB eurjchem-116 58 52     SPACE eurjchem-116 58 53 over over ADP eurjchem-116 58 54     SPACE eurjchem-116 58 55 a a DET eurjchem-116 58 56     SPACE eurjchem-116 58 57 period period NOUN eurjchem-116 58 58     SPACE eurjchem-116 58 59 of of ADP eurjchem-116 58 60     SPACE eurjchem-116 58 61 1 1 NUM eurjchem-116 58 62     SPACE eurjchem-116 58 63 month month NOUN eurjchem-116 58 64     SPACE eurjchem-116 58 65 did do AUX eurjchem-116 58 66     SPACE eurjchem-116 58 67 not not PART eurjchem-116 58 68     SPACE eurjchem-116 58 69 suffer suffer VERB eurjchem-116 58 70     SPACE eurjchem-116 58 71 any any DET eurjchem-116 58 72     SPACE eurjchem-116 58 73 appreciable appreciable ADJ eurjchem-116 58 74     SPACE eurjchem-116 58 75 changes change NOUN eurjchem-116 58 76     SPACE eurjchem-116 58 77 in in ADP eurjchem-116 58 78     SPACE eurjchem-116 58 79 assay assay NOUN eurjchem-116 58 80     SPACE eurjchem-116 58 81 value value NOUN eurjchem-116 58 82     SPACE eurjchem-116 58 83 and and CCONJ eurjchem-116 58 84     SPACE eurjchem-116 58 85 meet meet VERB eurjchem-116 58 86     SPACE eurjchem-116 58 87 the the DET eurjchem-116 58 88     SPACE eurjchem-116 58 89 criterion criterion NOUN eurjchem-116 58 90     SPACE eurjchem-116 58 91 mentioned mention VERB eurjchem-116 58 92     SPACE eurjchem-116 58 93 above above ADP eurjchem-116 58 94     SPACE eurjchem-116 58 95 and and CCONJ eurjchem-116 58 96     SPACE eurjchem-116 58 97 the the DET eurjchem-116 58 98     SPACE eurjchem-116 58 99 solutions solution NOUN eurjchem-116 58 100     SPACE eurjchem-116 58 101 were be AUX eurjchem-116 58 102     SPACE eurjchem-116 58 103 found find VERB eurjchem-116 58 104     SPACE eurjchem-116 58 105 to to PART eurjchem-116 58 106     SPACE eurjchem-116 58 107 be be AUX eurjchem-116 58 108     SPACE eurjchem-116 58 109 stable stable ADJ eurjchem-116 58 110     SPACE eurjchem-116 58 111 even even ADV eurjchem-116 58 112     SPACE eurjchem-116 58 113 after after ADP eurjchem-116 58 114     SPACE eurjchem-116 58 115 three three NUM eurjchem-116 58 116     SPACE eurjchem-116 58 117 freeze freeze NOUN eurjchem-116 58 118 – – PUNCT eurjchem-116 58 119 thaw thaw NOUN eurjchem-116 58 120     SPACE eurjchem-116 58 121 cycles cycle NOUN eurjchem-116 58 122     SPACE eurjchem-116 58 123 and and CCONJ eurjchem-116 58 124     SPACE eurjchem-116 58 125 the the DET eurjchem-116 58 126     SPACE eurjchem-116 58 127 results result NOUN eurjchem-116 58 128     SPACE eurjchem-116 58 129 were be AUX eurjchem-116 58 130     SPACE eurjchem-116 58 131 found find VERB eurjchem-116 58 132     SPACE eurjchem-116 58 133 to to PART eurjchem-116 58 134     SPACE eurjchem-116 58 135 be be AUX eurjchem-116 58 136     SPACE eurjchem-116 58 137 with with ADP eurjchem-116 58 138     SPACE eurjchem-116 58 139 the the DET eurjchem-116 58 140     SPACE eurjchem-116 58 141 range range NOUN eurjchem-116 58 142     SPACE eurjchem-116 58 143 of of ADP eurjchem-116 58 144     SPACE eurjchem-116 58 145 90‐110 90‐110 NUM eurjchem-116 58 146 % % NOUN eurjchem-116 58 147 . . PUNCT eurjchem-116 58 148                 SPACE eurjchem-116 59 1 3.2.6 3.2.6 NUM eurjchem-116 59 2 . . PUNCT eurjchem-116 59 3     SPACE eurjchem-116 59 4 system system NOUN eurjchem-116 59 5     SPACE eurjchem-116 59 6 suitability suitability NOUN eurjchem-116 59 7         SPACE eurjchem-116 59 8 system system NOUN eurjchem-116 59 9     SPACE eurjchem-116 59 10 suitability suitability NOUN eurjchem-116 59 11     SPACE eurjchem-116 59 12 tests test NOUN eurjchem-116 59 13 , , PUNCT eurjchem-116 59 14     SPACE eurjchem-116 59 15 an an DET eurjchem-116 59 16     SPACE eurjchem-116 59 17 integral integral ADJ eurjchem-116 59 18     SPACE eurjchem-116 59 19 part part NOUN eurjchem-116 59 20     SPACE eurjchem-116 59 21 of of ADP eurjchem-116 59 22     SPACE eurjchem-116 59 23 a a DET eurjchem-116 59 24     SPACE eurjchem-116 59 25 chromatographic chromatographic ADJ eurjchem-116 59 26     SPACE eurjchem-116 59 27 analysis analysis NOUN eurjchem-116 59 28     SPACE eurjchem-116 59 29 are be AUX eurjchem-116 59 30     SPACE eurjchem-116 59 31 used use VERB eurjchem-116 59 32     SPACE eurjchem-116 59 33 to to PART eurjchem-116 59 34     SPACE eurjchem-116 59 35 verify verify VERB eurjchem-116 59 36     SPACE eurjchem-116 59 37 that that SCONJ eurjchem-116 59 38     SPACE eurjchem-116 59 39 the the DET eurjchem-116 59 40     SPACE eurjchem-116 59 41 resolution resolution NOUN eurjchem-116 59 42     SPACE eurjchem-116 59 43 and and CCONJ eurjchem-116 59 44     SPACE eurjchem-116 59 45 reproducibility reproducibility NOUN eurjchem-116 59 46     SPACE eurjchem-116 59 47 of of ADP eurjchem-116 59 48     SPACE eurjchem-116 59 49 the the DET eurjchem-116 59 50     SPACE eurjchem-116 59 51 chromatographic chromatographic ADJ eurjchem-116 59 52     SPACE eurjchem-116 59 53 system system NOUN eurjchem-116 59 54     SPACE eurjchem-116 59 55 are be AUX eurjchem-116 59 56     SPACE eurjchem-116 59 57 adequate adequate ADJ eurjchem-116 59 58     SPACE eurjchem-116 59 59 for for ADP eurjchem-116 59 60     SPACE eurjchem-116 59 61 the the DET eurjchem-116 59 62     SPACE eurjchem-116 59 63 analysis analysis NOUN eurjchem-116 59 64 . . PUNCT eurjchem-116 59 65     SPACE eurjchem-116 60 1 a a DET eurjchem-116 60 2     SPACE eurjchem-116 60 3 system system NOUN eurjchem-116 60 4     SPACE eurjchem-116 60 5 suitability suitability NOUN eurjchem-116 60 6     SPACE eurjchem-116 60 7 test test NOUN eurjchem-116 60 8     SPACE eurjchem-116 60 9 according accord VERB eurjchem-116 60 10     SPACE eurjchem-116 60 11 to to PART eurjchem-116 60 12     SPACE eurjchem-116 60 13 usp usp NOUN eurjchem-116 60 14     SPACE eurjchem-116 60 15 was be AUX eurjchem-116 60 16     SPACE eurjchem-116 60 17 performed perform VERB eurjchem-116 60 18     SPACE eurjchem-116 60 19 on on ADP eurjchem-116 60 20     SPACE eurjchem-116 60 21 the the DET eurjchem-116 60 22     SPACE eurjchem-116 60 23 chromatograms chromatogram NOUN eurjchem-116 60 24     SPACE eurjchem-116 60 25 obtained obtain VERB eurjchem-116 60 26     SPACE eurjchem-116 60 27 from from ADP eurjchem-116 60 28     SPACE eurjchem-116 60 29 standard standard NOUN eurjchem-116 60 30     SPACE eurjchem-116 60 31 and and CCONJ eurjchem-116 60 32     SPACE eurjchem-116 60 33 test test NOUN eurjchem-116 60 34     SPACE eurjchem-116 60 35 solutions solution NOUN eurjchem-116 60 36     SPACE eurjchem-116 60 37 to to PART eurjchem-116 60 38     SPACE eurjchem-116 60 39 check check VERB eurjchem-116 60 40     SPACE eurjchem-116 60 41 different different ADJ eurjchem-116 60 42     SPACE eurjchem-116 60 43 above above ADV eurjchem-116 60 44     SPACE eurjchem-116 60 45 mentioned mention VERB eurjchem-116 60 46     SPACE eurjchem-116 60 47 parameters parameter NOUN eurjchem-116 60 48     SPACE eurjchem-116 60 49 and and CCONJ eurjchem-116 60 50     SPACE eurjchem-116 60 51 the the DET eurjchem-116 60 52     SPACE eurjchem-116 60 53 results result NOUN eurjchem-116 60 54     SPACE eurjchem-116 60 55 obtained obtain VERB eurjchem-116 60 56     SPACE eurjchem-116 60 57 from from ADP eurjchem-116 60 58     SPACE eurjchem-116 60 59 six six NUM eurjchem-116 60 60     SPACE eurjchem-116 60 61 replicate replicate VERB eurjchem-116 60 62     SPACE eurjchem-116 60 63 injections injection NOUN eurjchem-116 60 64     SPACE eurjchem-116 60 65 of of ADP eurjchem-116 60 66     SPACE eurjchem-116 60 67 the the DET eurjchem-116 60 68     SPACE eurjchem-116 60 69 standard standard ADJ eurjchem-116 60 70     SPACE eurjchem-116 60 71 solution solution NOUN eurjchem-116 60 72     SPACE eurjchem-116 60 73 are be AUX eurjchem-116 60 74     SPACE eurjchem-116 60 75 summarized summarize VERB eurjchem-116 60 76     SPACE eurjchem-116 60 77 in in ADP eurjchem-116 60 78     SPACE eurjchem-116 60 79 the the DET eurjchem-116 60 80     SPACE eurjchem-116 60 81 table table NOUN eurjchem-116 60 82     SPACE eurjchem-116 60 83 2 2 NUM eurjchem-116 60 84 . . PUNCT eurjchem-116 60 85         SPACE eurjchem-116 60 86 table table NOUN eurjchem-116 60 87     SPACE eurjchem-116 60 88 2 2 NUM eurjchem-116 60 89 . . PUNCT eurjchem-116 60 90     SPACE eurjchem-116 60 91 system system NOUN eurjchem-116 60 92     SPACE eurjchem-116 60 93 suitability suitability NOUN eurjchem-116 60 94     SPACE eurjchem-116 60 95 parameters parameter NOUN eurjchem-116 60 96 . . PUNCT eurjchem-116 60 97     SPACE eurjchem-116 61 1 parameter parameter NOUN eurjchem-116 61 2                     SPACE eurjchem-116 61 3 obtained obtain VERB eurjchem-116 61 4     SPACE eurjchem-116 61 5 value value NOUN eurjchem-116 61 6 * * NOUN eurjchem-116 61 7     SPACE eurjchem-116 61 8 retention retention NOUN eurjchem-116 61 9     SPACE eurjchem-116 61 10 time time NOUN eurjchem-116 61 11 , , PUNCT eurjchem-116 61 12     SPACE eurjchem-116 61 13 rt rt PROPN eurjchem-116 61 14 ( ( PUNCT eurjchem-116 61 15 min min PROPN eurjchem-116 61 16 ) ) PUNCT eurjchem-116 61 17                                                               SPACE eurjchem-116 61 18 3.264 3.264 NUM eurjchem-116 61 19     SPACE eurjchem-116 61 20 capacity capacity NOUN eurjchem-116 61 21     SPACE eurjchem-116 61 22 factor factor NOUN eurjchem-116 61 23     SPACE eurjchem-116 61 24 ( ( PUNCT eurjchem-116 61 25 k k NOUN eurjchem-116 61 26 ’ ' PUNCT eurjchem-116 61 27 ) ) PUNCT eurjchem-116 61 28                                                                                   SPACE eurjchem-116 61 29 4.834 4.834 NUM eurjchem-116 61 30     SPACE eurjchem-116 61 31 theoretical theoretical ADJ eurjchem-116 61 32     SPACE eurjchem-116 61 33 plates plate NOUN eurjchem-116 61 34     SPACE eurjchem-116 61 35 ( ( PUNCT eurjchem-116 61 36 usp usp NOUN eurjchem-116 61 37 ) ) PUNCT eurjchem-116 61 38                                                               SPACE eurjchem-116 61 39 7928 7928 NUM eurjchem-116 61 40       SPACE eurjchem-116 61 41 tailing tail VERB eurjchem-116 61 42     SPACE eurjchem-116 61 43 factor factor NOUN eurjchem-116 61 44     SPACE eurjchem-116 61 45 ( ( PUNCT eurjchem-116 61 46 tf tf PROPN eurjchem-116 61 47 ) ) PUNCT eurjchem-116 61 48                                                                                         SPACE eurjchem-116 61 49 1.15 1.15 NUM eurjchem-116 61 50     SPACE eurjchem-116 61 51 * * NUM eurjchem-116 61 52     SPACE eurjchem-116 61 53 average average NOUN eurjchem-116 61 54     SPACE eurjchem-116 61 55 of of ADP eurjchem-116 61 56     SPACE eurjchem-116 61 57 six six NUM eurjchem-116 61 58     SPACE eurjchem-116 61 59 determination determination NOUN eurjchem-116 61 60 . . PUNCT eurjchem-116 61 61         SPACE eurjchem-116 61 62 3.3 3.3 NUM eurjchem-116 61 63 . . PUNCT eurjchem-116 61 64     SPACE eurjchem-116 61 65 recovery recovery NOUN eurjchem-116 61 66     SPACE eurjchem-116 61 67 of of ADP eurjchem-116 61 68     SPACE eurjchem-116 61 69 voglibose voglibose NOUN eurjchem-116 61 70     SPACE eurjchem-116 61 71 from from ADP eurjchem-116 61 72     SPACE eurjchem-116 61 73 formulations formulation NOUN eurjchem-116 61 74         SPACE eurjchem-116 61 75 extraction extraction NOUN eurjchem-116 61 76     SPACE eurjchem-116 61 77 efficiency efficiency NOUN eurjchem-116 61 78     SPACE eurjchem-116 61 79 was be AUX eurjchem-116 61 80     SPACE eurjchem-116 61 81 performed perform VERB eurjchem-116 61 82     SPACE eurjchem-116 61 83 to to PART eurjchem-116 61 84     SPACE eurjchem-116 61 85 verify verify VERB eurjchem-116 61 86     SPACE eurjchem-116 61 87 the the DET eurjchem-116 61 88     SPACE eurjchem-116 61 89 effectiveness effectiveness NOUN eurjchem-116 61 90     SPACE eurjchem-116 61 91 of of ADP eurjchem-116 61 92     SPACE eurjchem-116 61 93 the the DET eurjchem-116 61 94     SPACE eurjchem-116 61 95 extraction extraction NOUN eurjchem-116 61 96     SPACE eurjchem-116 61 97 step step NOUN eurjchem-116 61 98     SPACE eurjchem-116 61 99 and and CCONJ eurjchem-116 61 100     SPACE eurjchem-116 61 101 the the DET eurjchem-116 61 102     SPACE eurjchem-116 61 103 accuracy accuracy NOUN eurjchem-116 61 104     SPACE eurjchem-116 61 105 of of ADP eurjchem-116 61 106     SPACE eurjchem-116 61 107 the the DET eurjchem-116 61 108     SPACE eurjchem-116 61 109 proposed propose VERB eurjchem-116 61 110     SPACE eurjchem-116 61 111 method method NOUN eurjchem-116 61 112 . . PUNCT eurjchem-116 61 113     SPACE eurjchem-116 62 1 the the DET eurjchem-116 62 2     SPACE eurjchem-116 62 3 extraction extraction NOUN eurjchem-116 62 4     SPACE eurjchem-116 62 5 efficiency efficiency NOUN eurjchem-116 62 6     SPACE eurjchem-116 62 7 of of ADP eurjchem-116 62 8     SPACE eurjchem-116 62 9 vgb vgb NOUN eurjchem-116 62 10     SPACE eurjchem-116 62 11 from from ADP eurjchem-116 62 12     SPACE eurjchem-116 62 13 formulation formulation NOUN eurjchem-116 62 14     SPACE eurjchem-116 62 15 samples sample NOUN eurjchem-116 62 16     SPACE eurjchem-116 62 17 was be AUX eurjchem-116 62 18     SPACE eurjchem-116 62 19 satisfactorily satisfactorily ADV eurjchem-116 62 20     SPACE eurjchem-116 62 21 ranged range VERB eurjchem-116 62 22     SPACE eurjchem-116 62 23 from from ADP eurjchem-116 62 24     SPACE eurjchem-116 62 25 98.35 98.35 NUM eurjchem-116 62 26     SPACE eurjchem-116 62 27 to to ADP eurjchem-116 62 28     SPACE eurjchem-116 62 29 100.62 100.62 NUM eurjchem-116 62 30     SPACE eurjchem-116 62 31 % % NOUN eurjchem-116 62 32     SPACE eurjchem-116 62 33 ( ( PUNCT eurjchem-116 62 34 r.s.d r.s.d NOUN eurjchem-116 62 35 . . PUNCT eurjchem-116 62 36     SPACE eurjchem-116 62 37 was be AUX eurjchem-116 62 38     SPACE eurjchem-116 62 39 less less ADJ eurjchem-116 62 40     SPACE eurjchem-116 62 41 than than ADP eurjchem-116 62 42     SPACE eurjchem-116 62 43 1.55 1.55 NUM eurjchem-116 62 44 ) ) PUNCT eurjchem-116 62 45     SPACE eurjchem-116 62 46 at at ADP eurjchem-116 62 47     SPACE eurjchem-116 62 48 all all DET eurjchem-116 62 49     SPACE eurjchem-116 62 50 three three NUM eurjchem-116 62 51     SPACE eurjchem-116 62 52 concentration concentration NOUN eurjchem-116 62 53     SPACE eurjchem-116 62 54 levels level NOUN eurjchem-116 62 55 , , PUNCT eurjchem-116 62 56     SPACE eurjchem-116 62 57 which which PRON eurjchem-116 62 58     SPACE eurjchem-116 62 59 confirm confirm VERB eurjchem-116 62 60     SPACE eurjchem-116 62 61 no no DET eurjchem-116 62 62     SPACE eurjchem-116 62 63 interference interference NOUN eurjchem-116 62 64     SPACE eurjchem-116 62 65 effects effect NOUN eurjchem-116 62 66     SPACE eurjchem-116 62 67 due due ADJ eurjchem-116 62 68     SPACE eurjchem-116 62 69 to to PART eurjchem-116 62 70     SPACE eurjchem-116 62 71 formulation formulation NOUN eurjchem-116 62 72     SPACE eurjchem-116 62 73 excipients excipient NOUN eurjchem-116 62 74     SPACE eurjchem-116 62 75 ( ( PUNCT eurjchem-116 62 76 table table NOUN eurjchem-116 62 77     SPACE eurjchem-116 62 78 3 3 NUM eurjchem-116 62 79 ) ) PUNCT eurjchem-116 62 80 . . PUNCT eurjchem-116 62 81           SPACE eurjchem-116 63 1 table table NOUN eurjchem-116 63 2     SPACE eurjchem-116 63 3 3 3 NUM eurjchem-116 63 4 . . PUNCT eurjchem-116 63 5     SPACE eurjchem-116 63 6 results result VERB eurjchem-116 63 7     SPACE eurjchem-116 63 8 of of ADP eurjchem-116 63 9     SPACE eurjchem-116 63 10 voglibose voglibose NOUN eurjchem-116 63 11     SPACE eurjchem-116 63 12 recovery recovery NOUN eurjchem-116 63 13     SPACE eurjchem-116 63 14 from from ADP eurjchem-116 63 15     SPACE eurjchem-116 63 16 formulations formulation NOUN eurjchem-116 63 17 . . PUNCT eurjchem-116 63 18     SPACE eurjchem-116 63 19 formulation formulation NOUN eurjchem-116 63 20     SPACE eurjchem-116 63 21 label label NOUN eurjchem-116 63 22     SPACE eurjchem-116 63 23 claim claim NOUN eurjchem-116 63 24     SPACE eurjchem-116 63 25 ( ( PUNCT eurjchem-116 63 26 mg mg ADJ eurjchem-116 63 27 ) ) PUNCT eurjchem-116 63 28         SPACE eurjchem-116 63 29 amount amount NOUN eurjchem-116 63 30     SPACE eurjchem-116 63 31 recovered recover VERB eurjchem-116 63 32     SPACE eurjchem-116 63 33 ( ( PUNCT eurjchem-116 63 34 mg mg ADJ eurjchem-116 63 35 ) ) PUNCT eurjchem-116 63 36                 SPACE eurjchem-116 63 37 percent percent NOUN eurjchem-116 63 38     SPACE eurjchem-116 63 39 recovery recovery NOUN eurjchem-116 63 40                   SPACE eurjchem-116 63 41 % % NOUN eurjchem-116 63 42     SPACE eurjchem-116 63 43 r.s.d r.s.d NOUN eurjchem-116 63 44 . . PUNCT eurjchem-116 63 45       SPACE eurjchem-116 64 1 volix volix PROPN eurjchem-116 64 2     SPACE eurjchem-116 64 3 ( ( PUNCT eurjchem-116 64 4 ranbaxy ranbaxy PROPN eurjchem-116 64 5 ) ) PUNCT eurjchem-116 64 6                         SPACE eurjchem-116 64 7 0.3 0.3 NUM eurjchem-116 64 8                                     SPACE eurjchem-116 64 9 0.297 0.297 NUM eurjchem-116 64 10                                               SPACE eurjchem-116 64 11 99.0 99.0 NUM eurjchem-116 64 12                                         SPACE eurjchem-116 64 13 1.37 1.37 NUM eurjchem-116 64 14     SPACE eurjchem-116 64 15 volix volix NOUN eurjchem-116 64 16     SPACE eurjchem-116 64 17 ( ( PUNCT eurjchem-116 64 18 ranbaxy ranbaxy PROPN eurjchem-116 64 19 ) ) PUNCT eurjchem-116 64 20                         SPACE eurjchem-116 64 21 0.2 0.2 NUM eurjchem-116 64 22                                     SPACE eurjchem-116 64 23 0.199 0.199 NUM eurjchem-116 64 24                                               SPACE eurjchem-116 64 25 99.5 99.5 NUM eurjchem-116 64 26                                         SPACE eurjchem-116 64 27 1.71 1.71 NUM eurjchem-116 64 28     SPACE eurjchem-116 64 29 voglitor voglitor NOUN eurjchem-116 64 30     SPACE eurjchem-116 64 31 ( ( PUNCT eurjchem-116 64 32 torrent torrent PROPN eurjchem-116 64 33 ) ) PUNCT eurjchem-116 64 34                     SPACE eurjchem-116 64 35 0.3 0.3 NUM eurjchem-116 64 36                                     SPACE eurjchem-116 64 37 0.295 0.295 NUM eurjchem-116 64 38                                               SPACE eurjchem-116 64 39 98.3 98.3 NUM eurjchem-116 64 40                                         SPACE eurjchem-116 64 41 2.06 2.06 NUM eurjchem-116 64 42       SPACE eurjchem-116 64 43 vocarb vocarb NOUN eurjchem-116 64 44     SPACE eurjchem-116 64 45 ( ( PUNCT eurjchem-116 64 46 glenmark glenmark PROPN eurjchem-116 64 47 ) ) PUNCT eurjchem-116 64 48                 SPACE eurjchem-116 64 49 0.2 0.2 NUM eurjchem-116 64 50                                     SPACE eurjchem-116 64 51 0.201 0.201 NUM eurjchem-116 64 52                                               SPACE eurjchem-116 64 53 100.5 100.5 NUM eurjchem-116 64 54                                     SPACE eurjchem-116 64 55 2.11 2.11 NUM eurjchem-116 64 56                                     SPACE eurjchem-116 64 57 4 4 NUM eurjchem-116 64 58 . . PUNCT eurjchem-116 64 59     SPACE eurjchem-116 64 60 conclusion conclusion NOUN eurjchem-116 64 61         SPACE eurjchem-116 64 62 in in ADP eurjchem-116 64 63     SPACE eurjchem-116 64 64 the the DET eurjchem-116 64 65     SPACE eurjchem-116 64 66 present present ADJ eurjchem-116 64 67     SPACE eurjchem-116 64 68 work work NOUN eurjchem-116 64 69 , , PUNCT eurjchem-116 64 70     SPACE eurjchem-116 64 71 a a DET eurjchem-116 64 72     SPACE eurjchem-116 64 73 new new ADJ eurjchem-116 64 74     SPACE eurjchem-116 64 75 rapid rapid ADJ eurjchem-116 64 76     SPACE eurjchem-116 64 77 and and CCONJ eurjchem-116 64 78     SPACE eurjchem-116 64 79 simple simple ADJ eurjchem-116 64 80     SPACE eurjchem-116 64 81 reverse reverse NOUN eurjchem-116 64 82     SPACE eurjchem-116 64 83 phase phase NOUN eurjchem-116 64 84     SPACE eurjchem-116 64 85 high high ADJ eurjchem-116 64 86     SPACE eurjchem-116 64 87 performance performance NOUN eurjchem-116 64 88     SPACE eurjchem-116 64 89 liquid liquid NOUN eurjchem-116 64 90     SPACE eurjchem-116 64 91 chromatographic chromatographic ADJ eurjchem-116 64 92     SPACE eurjchem-116 64 93 method method NOUN eurjchem-116 64 94     SPACE eurjchem-116 64 95 has have AUX eurjchem-116 64 96     SPACE eurjchem-116 64 97 been be AUX eurjchem-116 64 98     SPACE eurjchem-116 64 99 developed develop VERB eurjchem-116 64 100 , , PUNCT eurjchem-116 64 101     SPACE eurjchem-116 64 102 optimized optimize VERB eurjchem-116 64 103     SPACE eurjchem-116 64 104 and and CCONJ eurjchem-116 64 105     SPACE eurjchem-116 64 106 validated validate VERB eurjchem-116 64 107     SPACE eurjchem-116 64 108 for for ADP eurjchem-116 64 109     SPACE eurjchem-116 64 110 the the DET eurjchem-116 64 111     SPACE eurjchem-116 64 112 estimation estimation NOUN eurjchem-116 64 113     SPACE eurjchem-116 64 114 of of ADP eurjchem-116 64 115     SPACE eurjchem-116 64 116 voglibose voglibose NOUN eurjchem-116 64 117     SPACE eurjchem-116 64 118 in in ADP eurjchem-116 64 119     SPACE eurjchem-116 64 120 pharmaceutical pharmaceutical NOUN eurjchem-116 64 121     SPACE eurjchem-116 64 122 formulations formulation NOUN eurjchem-116 64 123     SPACE eurjchem-116 64 124 using use VERB eurjchem-116 64 125     SPACE eurjchem-116 64 126 refractive refractive ADJ eurjchem-116 64 127     SPACE eurjchem-116 64 128 index index NOUN eurjchem-116 64 129     SPACE eurjchem-116 64 130 detector detector NOUN eurjchem-116 64 131     SPACE eurjchem-116 64 132 and and CCONJ eurjchem-116 64 133     SPACE eurjchem-116 64 134 isocratic isocratic NOUN eurjchem-116 64 135     SPACE eurjchem-116 64 136 elution elution NOUN eurjchem-116 64 137 . . PUNCT eurjchem-116 64 138     SPACE eurjchem-116 65 1 the the DET eurjchem-116 65 2     SPACE eurjchem-116 65 3 short short ADJ eurjchem-116 65 4     SPACE eurjchem-116 65 5 peak peak NOUN eurjchem-116 65 6     SPACE eurjchem-116 65 7 retention retention NOUN eurjchem-116 65 8     SPACE eurjchem-116 65 9 time time NOUN eurjchem-116 65 10     SPACE eurjchem-116 65 11 of of ADP eurjchem-116 65 12     SPACE eurjchem-116 65 13 3.264 3.264 NUM eurjchem-116 65 14     SPACE eurjchem-116 65 15 min min NOUN eurjchem-116 65 16     SPACE eurjchem-116 65 17 cuts cut NOUN eurjchem-116 65 18     SPACE eurjchem-116 65 19 down down ADP eurjchem-116 65 20     SPACE eurjchem-116 65 21 on on ADP eurjchem-116 65 22     SPACE eurjchem-116 65 23 overall overall ADJ eurjchem-116 65 24     SPACE eurjchem-116 65 25 time time NOUN eurjchem-116 65 26     SPACE eurjchem-116 65 27 of of ADP eurjchem-116 65 28     SPACE eurjchem-116 65 29 sample sample NOUN eurjchem-116 65 30     SPACE eurjchem-116 65 31 analysis analysis NOUN eurjchem-116 65 32     SPACE eurjchem-116 65 33 and and CCONJ eurjchem-116 65 34     SPACE eurjchem-116 65 35 the the DET eurjchem-116 65 36     SPACE eurjchem-116 65 37 method method NOUN eurjchem-116 65 38     SPACE eurjchem-116 65 39 was be AUX eurjchem-116 65 40     SPACE eurjchem-116 65 41 more more ADJ eurjchem-116 65 42     SPACE eurjchem-116 65 43 cost cost NOUN eurjchem-116 65 44     SPACE eurjchem-116 65 45 effective effective ADJ eurjchem-116 65 46     SPACE eurjchem-116 65 47 as as SCONJ eurjchem-116 65 48     SPACE eurjchem-116 65 49 it it PRON eurjchem-116 65 50     SPACE eurjchem-116 65 51 utilizes utilize VERB eurjchem-116 65 52     SPACE eurjchem-116 65 53 very very ADV eurjchem-116 65 54     SPACE eurjchem-116 65 55 less less ADJ eurjchem-116 65 56     SPACE eurjchem-116 65 57 quantity quantity NOUN eurjchem-116 65 58     SPACE eurjchem-116 65 59 of of ADP eurjchem-116 65 60     SPACE eurjchem-116 65 61 mobile mobile ADJ eurjchem-116 65 62     SPACE eurjchem-116 65 63 phase phase NOUN eurjchem-116 65 64 . . PUNCT eurjchem-116 65 65     SPACE eurjchem-116 66 1 linearity linearity NOUN eurjchem-116 66 2     SPACE eurjchem-116 66 3 was be AUX eurjchem-116 66 4     SPACE eurjchem-116 66 5 found find VERB eurjchem-116 66 6     SPACE eurjchem-116 66 7 in in ADP eurjchem-116 66 8     SPACE eurjchem-116 66 9 a a DET eurjchem-116 66 10     SPACE eurjchem-116 66 11 range range NOUN eurjchem-116 66 12     SPACE eurjchem-116 66 13 of of ADP eurjchem-116 66 14     SPACE eurjchem-116 66 15 10‐ 10‐ NUM eurjchem-116 66 16 100 100 NUM eurjchem-116 66 17     SPACE eurjchem-116 66 18 µg µg VERB eurjchem-116 66 19 / / SYM eurjchem-116 66 20 ml ml VERB eurjchem-116 66 21     SPACE eurjchem-116 66 22 with with ADP eurjchem-116 66 23     SPACE eurjchem-116 66 24 lod lod NOUN eurjchem-116 66 25     SPACE eurjchem-116 66 26 and and CCONJ eurjchem-116 66 27     SPACE eurjchem-116 66 28 loq loq PROPN eurjchem-116 66 29     SPACE eurjchem-116 66 30 of of ADP eurjchem-116 66 31     SPACE eurjchem-116 66 32 2.91 2.91 NUM eurjchem-116 66 33     SPACE eurjchem-116 66 34 and and CCONJ eurjchem-116 66 35     SPACE eurjchem-116 66 36 9.70 9.70 NUM eurjchem-116 66 37     SPACE eurjchem-116 66 38 µg µg NOUN eurjchem-116 66 39 / / SYM eurjchem-116 66 40 ml ml NOUN eurjchem-116 66 41 , , PUNCT eurjchem-116 66 42     SPACE eurjchem-116 66 43 respectively respectively ADV eurjchem-116 66 44 . . PUNCT eurjchem-116 66 45     SPACE eurjchem-116 67 1 the the DET eurjchem-116 67 2     SPACE eurjchem-116 67 3 results result NOUN eurjchem-116 67 4     SPACE eurjchem-116 67 5 of of ADP eurjchem-116 67 6     SPACE eurjchem-116 67 7 t‐test t‐test VERB eurjchem-116 67 8     SPACE eurjchem-116 67 9 applied apply VERB eurjchem-116 67 10     SPACE eurjchem-116 67 11 to to ADP eurjchem-116 67 12     SPACE eurjchem-116 67 13 accuracy accuracy NOUN eurjchem-116 67 14     SPACE eurjchem-116 67 15 and and CCONJ eurjchem-116 67 16     SPACE eurjchem-116 67 17 precision precision NOUN eurjchem-116 67 18     SPACE eurjchem-116 67 19 data datum NOUN eurjchem-116 67 20     SPACE eurjchem-116 67 21 enabled enable VERB eurjchem-116 67 22     SPACE eurjchem-116 67 23 the the DET eurjchem-116 67 24     SPACE eurjchem-116 67 25 conclusion conclusion NOUN eurjchem-116 67 26     SPACE eurjchem-116 67 27 that that SCONJ eurjchem-116 67 28     SPACE eurjchem-116 67 29 an an DET eurjchem-116 67 30     SPACE eurjchem-116 67 31 excellent excellent ADJ eurjchem-116 67 32     SPACE eurjchem-116 67 33 accuracy accuracy NOUN eurjchem-116 67 34     SPACE eurjchem-116 67 35 and and CCONJ eurjchem-116 67 36     SPACE eurjchem-116 67 37 high high ADJ eurjchem-116 67 38     SPACE eurjchem-116 67 39 precision precision NOUN eurjchem-116 67 40     SPACE eurjchem-116 67 41 was be AUX eurjchem-116 67 42     SPACE eurjchem-116 67 43 achieved achieve VERB eurjchem-116 67 44 . . PUNCT eurjchem-116 67 45     SPACE eurjchem-116 67 46 from from ADP eurjchem-116 67 47     SPACE eurjchem-116 67 48 the the DET eurjchem-116 67 49     SPACE eurjchem-116 67 50 extraction extraction NOUN eurjchem-116 67 51     SPACE eurjchem-116 67 52 efficiency efficiency NOUN eurjchem-116 67 53     SPACE eurjchem-116 67 54 data datum NOUN eurjchem-116 67 55 , , PUNCT eurjchem-116 67 56     SPACE eurjchem-116 67 57 the the DET eurjchem-116 67 58     SPACE eurjchem-116 67 59 recovery recovery NOUN eurjchem-116 67 60     SPACE eurjchem-116 67 61 of of ADP eurjchem-116 67 62     SPACE eurjchem-116 67 63 the the DET eurjchem-116 67 64     SPACE eurjchem-116 67 65 active active ADJ eurjchem-116 67 66     SPACE eurjchem-116 67 67 component component NOUN eurjchem-116 67 68     SPACE eurjchem-116 67 69 was be AUX eurjchem-116 67 70     SPACE eurjchem-116 67 71 found find VERB eurjchem-116 67 72     SPACE eurjchem-116 67 73 to to PART eurjchem-116 67 74     SPACE eurjchem-116 67 75 be be AUX eurjchem-116 67 76     SPACE eurjchem-116 67 77 quantitative quantitative ADJ eurjchem-116 67 78 . . PUNCT eurjchem-116 67 79     SPACE eurjchem-116 68 1 selectivity selectivity NOUN eurjchem-116 68 2     SPACE eurjchem-116 68 3 of of ADP eurjchem-116 68 4     SPACE eurjchem-116 68 5 the the DET eurjchem-116 68 6     SPACE eurjchem-116 68 7 method method NOUN eurjchem-116 68 8     SPACE eurjchem-116 68 9 was be AUX eurjchem-116 68 10     SPACE eurjchem-116 68 11 demonstrated demonstrate VERB eurjchem-116 68 12     SPACE eurjchem-116 68 13 by by ADP eurjchem-116 68 14     SPACE eurjchem-116 68 15 the the DET eurjchem-116 68 16     SPACE eurjchem-116 68 17 absence absence NOUN eurjchem-116 68 18     SPACE eurjchem-116 68 19 of of ADP eurjchem-116 68 20     SPACE eurjchem-116 68 21 any any DET eurjchem-116 68 22     SPACE eurjchem-116 68 23 interfering interfere VERB eurjchem-116 68 24     SPACE eurjchem-116 68 25 peaks peak NOUN eurjchem-116 68 26     SPACE eurjchem-116 68 27 from from ADP eurjchem-116 68 28     SPACE eurjchem-116 68 29 other other ADJ eurjchem-116 68 30     SPACE eurjchem-116 68 31 coexisting coexist VERB eurjchem-116 68 32     SPACE eurjchem-116 68 33 excipient excipient ADJ eurjchem-116 68 34     SPACE eurjchem-116 68 35 substances substance NOUN eurjchem-116 68 36     SPACE eurjchem-116 68 37 at at ADP eurjchem-116 68 38     SPACE eurjchem-116 68 39 the the DET eurjchem-116 68 40     SPACE eurjchem-116 68 41 retention retention NOUN eurjchem-116 68 42     SPACE eurjchem-116 68 43 time time NOUN eurjchem-116 68 44     SPACE eurjchem-116 68 45 of of ADP eurjchem-116 68 46     SPACE eurjchem-116 68 47 the the DET eurjchem-116 68 48     SPACE eurjchem-116 68 49 drug drug NOUN eurjchem-116 68 50 . . PUNCT eurjchem-116 68 51     SPACE eurjchem-116 69 1 hence hence ADV eurjchem-116 69 2     SPACE eurjchem-116 69 3 this this DET eurjchem-116 69 4     SPACE eurjchem-116 69 5 method method NOUN eurjchem-116 69 6     SPACE eurjchem-116 69 7 can can AUX eurjchem-116 69 8     SPACE eurjchem-116 69 9 be be AUX eurjchem-116 69 10     SPACE eurjchem-116 69 11 easily easily ADV eurjchem-116 69 12     SPACE eurjchem-116 69 13 and and CCONJ eurjchem-116 69 14     SPACE eurjchem-116 69 15 conveniently conveniently ADV eurjchem-116 69 16     SPACE eurjchem-116 69 17 used use VERB eurjchem-116 69 18     SPACE eurjchem-116 69 19 for for ADP eurjchem-116 69 20     SPACE eurjchem-116 69 21 the the DET eurjchem-116 69 22     SPACE eurjchem-116 69 23 routine routine ADJ eurjchem-116 69 24     SPACE eurjchem-116 69 25 analysis analysis NOUN eurjchem-116 69 26     SPACE eurjchem-116 69 27 of of ADP eurjchem-116 69 28     SPACE eurjchem-116 69 29 the the DET eurjchem-116 69 30     SPACE eurjchem-116 69 31 drug drug NOUN eurjchem-116 69 32     SPACE eurjchem-116 69 33 in in ADP eurjchem-116 69 34     SPACE eurjchem-116 69 35 pharmaceutical pharmaceutical NOUN eurjchem-116 69 36     SPACE eurjchem-116 69 37 formulations formulation NOUN eurjchem-116 69 38 . . PUNCT eurjchem-116 69 39         SPACE eurjchem-116 69 40 acknowledgement acknowledgement NOUN eurjchem-116 69 41         SPACE eurjchem-116 69 42 tirumala tirumala PROPN eurjchem-116 69 43     SPACE eurjchem-116 69 44 rajesh rajesh PROPN eurjchem-116 69 45     SPACE eurjchem-116 69 46 is be AUX eurjchem-116 69 47     SPACE eurjchem-116 69 48 grateful grateful ADJ eurjchem-116 69 49     SPACE eurjchem-116 69 50 to to ADP eurjchem-116 69 51     SPACE eurjchem-116 69 52 university university NOUN eurjchem-116 69 53     SPACE eurjchem-116 69 54 grants grant NOUN eurjchem-116 69 55     SPACE eurjchem-116 69 56 commission commission NOUN eurjchem-116 69 57     SPACE eurjchem-116 69 58 ( ( PUNCT eurjchem-116 69 59 ugc ugc PROPN eurjchem-116 69 60 ) ) PUNCT eurjchem-116 69 61 , , PUNCT eurjchem-116 69 62     SPACE eurjchem-116 69 63 new new ADJ eurjchem-116 69 64     SPACE eurjchem-116 69 65 delhi delhi ADJ eurjchem-116 69 66 , , PUNCT eurjchem-116 69 67     SPACE eurjchem-116 69 68 india india PROPN eurjchem-116 69 69     SPACE eurjchem-116 69 70 for for ADP eurjchem-116 69 71     SPACE eurjchem-116 69 72 providing provide VERB eurjchem-116 69 73     SPACE eurjchem-116 69 74 junior junior ADJ eurjchem-116 69 75     SPACE eurjchem-116 69 76 research research NOUN eurjchem-116 69 77     SPACE eurjchem-116 69 78 fellowship fellowship NOUN eurjchem-116 69 79     SPACE eurjchem-116 69 80 ( ( PUNCT eurjchem-116 69 81 jrf jrf PROPN eurjchem-116 69 82 ) ) PUNCT eurjchem-116 69 83     SPACE eurjchem-116 69 84 and and CCONJ eurjchem-116 69 85     SPACE eurjchem-116 69 86 to to PART eurjchem-116 69 87     SPACE eurjchem-116 69 88 dr dr PROPN eurjchem-116 69 89 . . PROPN eurjchem-116 69 90     SPACE eurjchem-116 69 91 r. r. PROPN eurjchem-116 69 92     SPACE eurjchem-116 69 93 shiva shiva PROPN eurjchem-116 69 94     SPACE eurjchem-116 69 95 kumar kumar PROPN eurjchem-116 69 96 , , PUNCT eurjchem-116 69 97     SPACE eurjchem-116 69 98 pro‐vice pro‐vice NOUN eurjchem-116 69 99     SPACE eurjchem-116 69 100 chancellor chancellor NOUN eurjchem-116 69 101 , , PUNCT eurjchem-116 69 102     SPACE eurjchem-116 69 103 srm srm PROPN eurjchem-116 69 104     SPACE eurjchem-116 69 105 university university NOUN eurjchem-116 69 106 , , PUNCT eurjchem-116 69 107     SPACE eurjchem-116 69 108 kattankulathur kattankulathur PROPN eurjchem-116 69 109     SPACE eurjchem-116 69 110 for for ADP eurjchem-116 69 111     SPACE eurjchem-116 69 112 providing provide VERB eurjchem-116 69 113     SPACE eurjchem-116 69 114 the the DET eurjchem-116 69 115     SPACE eurjchem-116 69 116 facilities facility NOUN eurjchem-116 69 117     SPACE eurjchem-116 69 118 to to PART eurjchem-116 69 119     SPACE eurjchem-116 69 120 carry carry VERB eurjchem-116 69 121     SPACE eurjchem-116 69 122 this this DET eurjchem-116 69 123     SPACE eurjchem-116 69 124 research research NOUN eurjchem-116 69 125     SPACE eurjchem-116 69 126 work work NOUN eurjchem-116 69 127 . . PUNCT eurjchem-116 69 128                 SPACE eurjchem-116 69 129 lakshmi lakshmi NOUN eurjchem-116 69 130     SPACE eurjchem-116 69 131 and and CCONJ eurjchem-116 69 132     SPACE eurjchem-116 69 133 rajesh rajesh PROPN eurjchem-116 69 134     SPACE eurjchem-116 69 135 / / SYM eurjchem-116 69 136     SPACE eurjchem-116 69 137 european european ADJ eurjchem-116 69 138     SPACE eurjchem-116 69 139 journal journal NOUN eurjchem-116 69 140     SPACE eurjchem-116 69 141 of of ADP eurjchem-116 69 142     SPACE eurjchem-116 69 143 chemistry chemistry NOUN eurjchem-116 69 144     SPACE eurjchem-116 69 145 1 1 NUM eurjchem-116 69 146     SPACE eurjchem-116 69 147 ( ( PUNCT eurjchem-116 69 148 4 4 NUM eurjchem-116 69 149 ) ) PUNCT eurjchem-116 69 150     SPACE eurjchem-116 69 151 ( ( PUNCT eurjchem-116 69 152 2010 2010 NUM eurjchem-116 69 153 ) ) PUNCT eurjchem-116 69 154     SPACE eurjchem-116 69 155 262­265 262­265 NOUN eurjchem-116 69 156     SPACE eurjchem-116 69 157 265 265 NUM eurjchem-116 69 158     SPACE eurjchem-116 69 159 references reference NOUN eurjchem-116 69 160         SPACE eurjchem-116 69 161 [ [ X eurjchem-116 69 162 1 1 NUM eurjchem-116 69 163 ] ] PUNCT eurjchem-116 69 164 . . PUNCT eurjchem-116 70 1 yamasaki yamasaki PROPN eurjchem-116 70 2 , , PUNCT eurjchem-116 70 3     SPACE eurjchem-116 70 4 y. y. NOUN eurjchem-116 70 5 ; ; PUNCT eurjchem-116 70 6     SPACE eurjchem-116 70 7 katakami katakami NOUN eurjchem-116 70 8 , , PUNCT eurjchem-116 70 9     SPACE eurjchem-116 70 10 n. n. NOUN eurjchem-116 70 11 ; ; PUNCT eurjchem-116 70 12     SPACE eurjchem-116 70 13 hayaishi‐okano hayaishi‐okano PROPN eurjchem-116 70 14 , , PUNCT eurjchem-116 70 15     SPACE eurjchem-116 70 16 r. r. PROPN eurjchem-116 70 17 ; ; PUNCT eurjchem-116 70 18     SPACE eurjchem-116 70 19 matsuhisa matsuhisa NOUN eurjchem-116 70 20 , , PUNCT eurjchem-116 70 21     SPACE eurjchem-116 70 22 m. m. NOUN eurjchem-116 70 23 ; ; PUNCT eurjchem-116 70 24     SPACE eurjchem-116 70 25 kajimoto kajimoto NOUN eurjchem-116 70 26 , , PUNCT eurjchem-116 70 27     SPACE eurjchem-116 70 28 y. y. NOUN eurjchem-116 70 29 ; ; PUNCT eurjchem-116 70 30     SPACE eurjchem-116 70 31 kosugi kosugi NOUN eurjchem-116 70 32 , , PUNCT eurjchem-116 70 33     SPACE eurjchem-116 70 34 k. k. PROPN eurjchem-116 70 35 ; ; PUNCT eurjchem-116 70 36     SPACE eurjchem-116 70 37 hatano hatano NOUN eurjchem-116 70 38 , , PUNCT eurjchem-116 70 39     SPACE eurjchem-116 70 40 m. m. NOUN eurjchem-116 70 41 ; ; PUNCT eurjchem-116 70 42     SPACE eurjchem-116 70 43 hori hori PROPN eurjchem-116 70 44 , , PUNCT eurjchem-116 70 45     SPACE eurjchem-116 70 46 m. m. NOUN eurjchem-116 70 47     SPACE eurjchem-116 70 48 diabetes diabetes NOUN eurjchem-116 70 49     SPACE eurjchem-116 70 50 res re NOUN eurjchem-116 70 51 . . PUNCT eurjchem-116 70 52     SPACE eurjchem-116 70 53 clin clin PROPN eurjchem-116 70 54 . . PUNCT eurjchem-116 70 55     SPACE eurjchem-116 70 56 pract pract PROPN eurjchem-116 70 57 . . PUNCT eurjchem-116 70 58     SPACE eurjchem-116 70 59 2005 2005 NUM eurjchem-116 70 60 , , PUNCT eurjchem-116 70 61     SPACE eurjchem-116 70 62 67 67 NUM eurjchem-116 70 63 , , PUNCT eurjchem-116 70 64     SPACE eurjchem-116 70 65 204‐210 204‐210 NOUN eurjchem-116 70 66 . . PUNCT eurjchem-116 70 67     SPACE eurjchem-116 71 1 [ [ X eurjchem-116 71 2 2 2 NUM eurjchem-116 71 3 ] ] PUNCT eurjchem-116 71 4 . . PUNCT eurjchem-116 72 1 watanabe watanabe PROPN eurjchem-116 72 2 , , PUNCT eurjchem-116 72 3     SPACE eurjchem-116 72 4 k. k. PROPN eurjchem-116 72 5 ; ; PUNCT eurjchem-116 72 6     SPACE eurjchem-116 72 7 uchino uchino PROPN eurjchem-116 72 8 , , PUNCT eurjchem-116 72 9     SPACE eurjchem-116 72 10 h. h. PROPN eurjchem-116 72 11 ; ; PUNCT eurjchem-116 72 12     SPACE eurjchem-116 72 13 ohmura ohmura NOUN eurjchem-116 72 14 , , PUNCT eurjchem-116 72 15     SPACE eurjchem-116 72 16 c. c. NOUN eurjchem-116 72 17 ; ; PUNCT eurjchem-116 72 18     SPACE eurjchem-116 72 19 tanaka tanaka PROPN eurjchem-116 72 20 , , PUNCT eurjchem-116 72 21     SPACE eurjchem-116 72 22 y. y. NOUN eurjchem-116 72 23 ; ; PUNCT eurjchem-116 72 24     SPACE eurjchem-116 72 25 onuma onuma ADJ eurjchem-116 72 26 , , PUNCT eurjchem-116 72 27     SPACE eurjchem-116 72 28 t. t. NOUN eurjchem-116 72 29 ; ; PUNCT eurjchem-116 72 30     SPACE eurjchem-116 72 31 kawamori kawamori X eurjchem-116 72 32 , , PUNCT eurjchem-116 72 33     SPACE eurjchem-116 72 34 r. r. PROPN eurjchem-116 72 35     SPACE eurjchem-116 72 36 j. j. PROPN eurjchem-116 72 37     SPACE eurjchem-116 72 38 diabetes diabetes PROPN eurjchem-116 72 39     SPACE eurjchem-116 72 40 complicat complicat NOUN eurjchem-116 72 41 . . PUNCT eurjchem-116 72 42     SPACE eurjchem-116 72 43 2004 2004 NUM eurjchem-116 72 44 , , PUNCT eurjchem-116 72 45     SPACE eurjchem-116 72 46 18 18 NUM eurjchem-116 72 47 , , PUNCT eurjchem-116 72 48     SPACE eurjchem-116 72 49 183‐186 183‐186 NUM eurjchem-116 72 50 . . PUNCT eurjchem-116 72 51     SPACE eurjchem-116 73 1 [ [ X eurjchem-116 73 2 3 3 NUM eurjchem-116 73 3 ] ] PUNCT eurjchem-116 73 4 . . PUNCT eurjchem-116 73 5 vichayanrat vichayanrat PROPN eurjchem-116 73 6 , , PUNCT eurjchem-116 73 7     SPACE eurjchem-116 73 8 a. a. NOUN eurjchem-116 73 9 ; ; PUNCT eurjchem-116 73 10     SPACE eurjchem-116 73 11 ploybutr ploybutr NOUN eurjchem-116 73 12 , , PUNCT eurjchem-116 73 13     SPACE eurjchem-116 73 14 s. s. PROPN eurjchem-116 73 15 ; ; PUNCT eurjchem-116 73 16     SPACE eurjchem-116 73 17 tunlakit tunlakit ADJ eurjchem-116 73 18 , , PUNCT eurjchem-116 73 19     SPACE eurjchem-116 73 20 m. m. NOUN eurjchem-116 73 21 ; ; PUNCT eurjchem-116 73 22     SPACE eurjchem-116 73 23 watanakejorn watanakejorn ADJ eurjchem-116 73 24 , , PUNCT eurjchem-116 73 25     SPACE eurjchem-116 73 26 p. p. NOUN eurjchem-116 73 27     SPACE eurjchem-116 73 28 diabetes diabete NOUN eurjchem-116 73 29     SPACE eurjchem-116 73 30 res re NOUN eurjchem-116 73 31 . . PUNCT eurjchem-116 73 32     SPACE eurjchem-116 73 33 clin clin PROPN eurjchem-116 73 34 . . PUNCT eurjchem-116 73 35     SPACE eurjchem-116 73 36 pract pract PROPN eurjchem-116 73 37 . . PUNCT eurjchem-116 73 38     SPACE eurjchem-116 74 1 2002 2002 NUM eurjchem-116 74 2 , , PUNCT eurjchem-116 74 3     SPACE eurjchem-116 74 4 55 55 NUM eurjchem-116 74 5 , , PUNCT eurjchem-116 74 6     SPACE eurjchem-116 74 7 99‐103 99‐103 NUM eurjchem-116 74 8 . . PUNCT eurjchem-116 74 9     SPACE eurjchem-116 75 1 [ [ X eurjchem-116 75 2 4 4 NUM eurjchem-116 75 3 ] ] PUNCT eurjchem-116 75 4 . . PUNCT eurjchem-116 76 1 zhang zhang PROPN eurjchem-116 76 2 , , PUNCT eurjchem-116 76 3     SPACE eurjchem-116 76 4 h. h. PROPN eurjchem-116 76 5 ; ; PUNCT eurjchem-116 76 6     SPACE eurjchem-116 76 7 sun sun NOUN eurjchem-116 76 8 , , PUNCT eurjchem-116 76 9     SPACE eurjchem-116 76 10 c. c. PROPN eurjchem-116 76 11     SPACE eurjchem-116 76 12 r. r. PROPN eurjchem-116 76 13 ; ; PUNCT eurjchem-116 76 14     SPACE eurjchem-116 76 15 ishurd ishurd VERB eurjchem-116 76 16 , , PUNCT eurjchem-116 76 17     SPACE eurjchem-116 76 18 o. o. PROPN eurjchem-116 76 19 ; ; PUNCT eurjchem-116 76 20     SPACE eurjchem-116 76 21 pan pan NOUN eurjchem-116 76 22 , , PUNCT eurjchem-116 76 23     SPACE eurjchem-116 76 24 y.j y.j PROPN eurjchem-116 76 25 . . PROPN eurjchem-116 76 26 ; ; PUNCT eurjchem-116 76 27     SPACE eurjchem-116 76 28 ding ding NOUN eurjchem-116 76 29 , , PUNCT eurjchem-116 76 30     SPACE eurjchem-116 76 31 l.s l.s PROPN eurjchem-116 76 32 . . NOUN eurjchem-116 76 33     SPACE eurjchem-116 76 34 carbohydr carbohydr NOUN eurjchem-116 76 35 . . PUNCT eurjchem-116 76 36     SPACE eurjchem-116 76 37 res re NOUN eurjchem-116 76 38 . . PUNCT eurjchem-116 76 39     SPACE eurjchem-116 76 40 2004 2004 NUM eurjchem-116 76 41 , , PUNCT eurjchem-116 76 42     SPACE eurjchem-116 76 43 339 339 NUM eurjchem-116 76 44 , , PUNCT eurjchem-116 76 45     SPACE eurjchem-116 76 46 2027‐2030 2027‐2030 NUM eurjchem-116 76 47 . . PUNCT eurjchem-116 76 48     SPACE eurjchem-116 77 1 [ [ X eurjchem-116 77 2 5 5 NUM eurjchem-116 77 3 ] ] PUNCT eurjchem-116 77 4 . . PUNCT eurjchem-116 78 1 chen chen PROPN eurjchem-116 78 2 , , PUNCT eurjchem-116 78 3     SPACE eurjchem-116 78 4 x. x. NOUN eurjchem-116 78 5 ; ; PUNCT eurjchem-116 78 6     SPACE eurjchem-116 78 7 zheng zheng PROPN eurjchem-116 78 8 , , PUNCT eurjchem-116 78 9     SPACE eurjchem-116 78 10 y. y. PROPN eurjchem-116 78 11 ; ; PUNCT eurjchem-116 78 12     SPACE eurjchem-116 78 13 shen shen NOUN eurjchem-116 78 14 , , PUNCT eurjchem-116 78 15     SPACE eurjchem-116 78 16 y. y. NOUN eurjchem-116 78 17     SPACE eurjchem-116 78 18 curr curr PROPN eurjchem-116 78 19 . . PUNCT eurjchem-116 78 20     SPACE eurjchem-116 78 21 med med PROPN eurjchem-116 78 22 . . PUNCT eurjchem-116 78 23     SPACE eurjchem-116 78 24 chem chem NOUN eurjchem-116 78 25 . . PUNCT eurjchem-116 78 26     SPACE eurjchem-116 78 27 2006 2006 NUM eurjchem-116 78 28 , , PUNCT eurjchem-116 78 29     SPACE eurjchem-116 78 30 13 13 NUM eurjchem-116 78 31 , , PUNCT eurjchem-116 78 32     SPACE eurjchem-116 78 33 109‐116 109‐116 NUM eurjchem-116 78 34 . . PUNCT eurjchem-116 78 35     SPACE eurjchem-116 79 1 [ [ X eurjchem-116 79 2 6 6 NUM eurjchem-116 79 3 ] ] PUNCT eurjchem-116 79 4 . . PUNCT eurjchem-116 79 5 rethfeld rethfeld VERB eurjchem-116 79 6 , , PUNCT eurjchem-116 79 7     SPACE eurjchem-116 79 8 i. i. NOUN eurjchem-116 79 9 ; ; PUNCT eurjchem-116 79 10     SPACE eurjchem-116 79 11 blaschke blaschke ADJ eurjchem-116 79 12 , , PUNCT eurjchem-116 79 13     SPACE eurjchem-116 79 14 g. g. PROPN eurjchem-116 79 15     SPACE eurjchem-116 79 16 j. j. PROPN eurjchem-116 79 17     SPACE eurjchem-116 79 18 chromatogr chromatogr PROPN eurjchem-116 79 19 . . PUNCT eurjchem-116 79 20     SPACE eurjchem-116 80 1 b b X eurjchem-116 80 2     SPACE eurjchem-116 80 3 1997 1997 NUM eurjchem-116 80 4 , , PUNCT eurjchem-116 80 5     SPACE eurjchem-116 80 6 700 700 NUM eurjchem-116 80 7 , , PUNCT eurjchem-116 80 8     SPACE eurjchem-116 80 9 249‐253 249‐253 NUM eurjchem-116 80 10 . . PUNCT eurjchem-116 80 11     SPACE eurjchem-116 81 1 [ [ X eurjchem-116 81 2 7 7 NUM eurjchem-116 81 3 ] ] PUNCT eurjchem-116 81 4 . . PUNCT eurjchem-116 81 5 woo woo AUX eurjchem-116 81 6 . . PUNCT eurjchem-116 81 7     SPACE eurjchem-116 81 8 j. j. PROPN eurjchem-116 81 9     SPACE eurjchem-116 81 10 s. s. PROPN eurjchem-116 81 11 ; ; PUNCT eurjchem-116 81 12     SPACE eurjchem-116 81 13 ryu ryu ADJ eurjchem-116 81 14 , , PUNCT eurjchem-116 81 15     SPACE eurjchem-116 81 16 j. j. PROPN eurjchem-116 81 17     SPACE eurjchem-116 81 18 k. k. PROPN eurjchem-116 81 19     SPACE eurjchem-116 81 20 j. j. PROPN eurjchem-116 81 21     SPACE eurjchem-116 81 22 pharm pharm PROPN eurjchem-116 81 23 . . PUNCT eurjchem-116 81 24     SPACE eurjchem-116 81 25 biomed biome VERB eurjchem-116 81 26 . . PUNCT eurjchem-116 81 27     SPACE eurjchem-116 82 1 anal anal ADJ eurjchem-116 82 2 . . PUNCT eurjchem-116 82 3     SPACE eurjchem-116 83 1 2006 2006 NUM eurjchem-116 83 2 , , PUNCT eurjchem-116 83 3     SPACE eurjchem-116 83 4 42 42 NUM eurjchem-116 83 5 , , PUNCT eurjchem-116 83 6     SPACE eurjchem-116 83 7 328‐333 328‐333 NUM eurjchem-116 83 8 . . PUNCT eurjchem-116 83 9     SPACE eurjchem-116 84 1 [ [ X eurjchem-116 84 2 8 8 NUM eurjchem-116 84 3 ] ] PUNCT eurjchem-116 84 4 . . PUNCT eurjchem-116 84 5 saiz‐abajo saiz‐abajo PROPN eurjchem-116 84 6 , , PUNCT eurjchem-116 84 7     SPACE eurjchem-116 84 8 m. m. NOUN eurjchem-116 84 9     SPACE eurjchem-116 84 10 j. j. PROPN eurjchem-116 84 11 ; ; PUNCT eurjchem-116 84 12     SPACE eurjchem-116 84 13 gonzalez‐saiz gonzalez‐saiz PROPN eurjchem-116 84 14 , , PUNCT eurjchem-116 84 15     SPACE eurjchem-116 84 16 j. j. PROPN eurjchem-116 84 17     SPACE eurjchem-116 84 18 m. m. NOUN eurjchem-116 84 19 ; ; PUNCT eurjchem-116 84 20     SPACE eurjchem-116 84 21 consuelo consuelo PROPN eurjchem-116 84 22 , , PUNCT eurjchem-116 84 23     SPACE eurjchem-116 84 24 p. p. NOUN eurjchem-116 84 25     SPACE eurjchem-116 84 26 anal anal NOUN eurjchem-116 84 27 . . PUNCT eurjchem-116 84 28     SPACE eurjchem-116 84 29 chim chim PROPN eurjchem-116 84 30 . . PUNCT eurjchem-116 84 31     SPACE eurjchem-116 84 32 acta acta PROPN eurjchem-116 84 33     SPACE eurjchem-116 84 34 2005 2005 NUM eurjchem-116 84 35 , , PUNCT eurjchem-116 84 36     SPACE eurjchem-116 84 37 528 528 NUM eurjchem-116 84 38 , , PUNCT eurjchem-116 84 39     SPACE eurjchem-116 84 40 63‐76 63‐76 NOUN eurjchem-116 84 41 . . PUNCT eurjchem-116 84 42     SPACE eurjchem-116 85 1 [ [ X eurjchem-116 85 2 9 9 NUM eurjchem-116 85 3 ] ] PUNCT eurjchem-116 85 4 . . PUNCT eurjchem-116 86 1 ich ich NOUN eurjchem-116 86 2     SPACE eurjchem-116 86 3 guidelines guideline NOUN eurjchem-116 86 4 , , PUNCT eurjchem-116 86 5     SPACE eurjchem-116 86 6 validation validation NOUN eurjchem-116 86 7     SPACE eurjchem-116 86 8 of of ADP eurjchem-116 86 9     SPACE eurjchem-116 86 10 analytical analytical ADJ eurjchem-116 86 11     SPACE eurjchem-116 86 12 procedures procedure NOUN eurjchem-116 86 13 : : PUNCT eurjchem-116 86 14     SPACE eurjchem-116 86 15 q2a q2a PROPN eurjchem-116 86 16 , , PUNCT eurjchem-116 86 17     SPACE eurjchem-116 86 18 1994 1994 NUM eurjchem-116 86 19 . . PUNCT eurjchem-116 86 20     SPACE eurjchem-116 87 1 [ [ X eurjchem-116 87 2 10 10 NUM eurjchem-116 87 3 ] ] PUNCT eurjchem-116 87 4 . . PUNCT eurjchem-116 88 1 ich ich NOUN eurjchem-116 88 2     SPACE eurjchem-116 88 3 guidelines guideline NOUN eurjchem-116 88 4 , , PUNCT eurjchem-116 88 5     SPACE eurjchem-116 88 6 validation validation NOUN eurjchem-116 88 7     SPACE eurjchem-116 88 8 of of ADP eurjchem-116 88 9     SPACE eurjchem-116 88 10 analytical analytical ADJ eurjchem-116 88 11     SPACE eurjchem-116 88 12 procedures procedure NOUN eurjchem-116 88 13 : : PUNCT eurjchem-116 88 14     SPACE eurjchem-116 88 15 q2b q2b NOUN eurjchem-116 88 16 , , PUNCT eurjchem-116 88 17     SPACE eurjchem-116 88 18 1996 1996 NUM eurjchem-116 88 19 . . PUNCT eurjchem-116 88 20     SPACE eurjchem-116 89 1 [ [ X eurjchem-116 89 2 11 11 NUM eurjchem-116 89 3 ] ] PUNCT eurjchem-116 89 4 . . PUNCT eurjchem-116 89 5 ich ich NOUN eurjchem-116 89 6     SPACE eurjchem-116 89 7 draft draft NOUN eurjchem-116 89 8     SPACE eurjchem-116 89 9 guidelines guideline NOUN eurjchem-116 89 10 , , PUNCT eurjchem-116 89 11     SPACE eurjchem-116 89 12 validation validation NOUN eurjchem-116 89 13     SPACE eurjchem-116 89 14 of of ADP eurjchem-116 89 15     SPACE eurjchem-116 89 16 analytical analytical ADJ eurjchem-116 89 17     SPACE eurjchem-116 89 18 procedures procedure NOUN eurjchem-116 89 19 : : PUNCT eurjchem-116 89 20     SPACE eurjchem-116 89 21 definitions definition NOUN eurjchem-116 89 22     SPACE eurjchem-116 89 23 and and CCONJ eurjchem-116 89 24     SPACE eurjchem-116 89 25 terminology terminology NOUN eurjchem-116 89 26 , , PUNCT eurjchem-116 89 27     SPACE eurjchem-116 89 28 federal federal ADJ eurjchem-116 89 29     SPACE eurjchem-116 89 30 register register VERB eurjchem-116 89 31 , , PUNCT eurjchem-116 89 32     SPACE eurjchem-116 89 33 vol vol NOUN eurjchem-116 89 34 . . PUNCT eurjchem-116 89 35     SPACE eurjchem-116 89 36 60 60 NUM eurjchem-116 89 37 , , PUNCT eurjchem-116 89 38     SPACE eurjchem-116 89 39 ifpma ifpma NOUN eurjchem-116 89 40 , , PUNCT eurjchem-116 89 41     SPACE eurjchem-116 89 42 switzerland switzerland PROPN eurjchem-116 89 43 , , PUNCT eurjchem-116 89 44     SPACE eurjchem-116 89 45 1995 1995 NUM eurjchem-116 89 46 . . PUNCT eurjchem-116 89 47     SPACE