id	sid	tid	token	lemma	pos
eurjchem-1251	1	1	untitled	untitle	VERB
eurjchem-1251	1	2	european	european	PROPN
eurjchem-1251	1	3	journal	journal	PROPN
eurjchem-1251	1	4	of	of	ADP
eurjchem-1251	1	5	chemistry	chemistry	NOUN
eurjchem-1251	1	6	6	6	NUM
eurjchem-1251	1	7	(	(	PUNCT
eurjchem-1251	1	8	2	2	NUM
eurjchem-1251	1	9	)	)	PUNCT
eurjchem-1251	1	10	(	(	PUNCT
eurjchem-1251	1	11	2015	2015	NUM
eurjchem-1251	1	12	)	)	PUNCT
eurjchem-1251	1	13	211‐218	211‐218	NUM
eurjchem-1251	1	14	european	european	ADJ
eurjchem-1251	1	15	journal	journal	PROPN
eurjchem-1251	1	16	of	of	ADP
eurjchem-1251	1	17	chemistry	chemistry	NOUN
eurjchem-1251	1	18	issn	issn	PROPN
eurjchem-1251	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-1251	1	20	(	(	PUNCT
eurjchem-1251	1	21	print	print	NOUN
eurjchem-1251	1	22	)	)	PUNCT
eurjchem-1251	1	23	/	/	SYM
eurjchem-1251	1	24	issn	issn	PROPN
eurjchem-1251	1	25	2153‐2257	2153‐2257	NUM
eurjchem-1251	1	26	(	(	PUNCT
eurjchem-1251	1	27	online	online	ADJ
eurjchem-1251	1	28	)	)	PUNCT
eurjchem-1251	1	29			NOUN
eurjchem-1251	1	30	2015	2015	NUM
eurjchem-1251	1	31	atlanta	atlanta	PROPN
eurjchem-1251	1	32	publishing	publishing	PROPN
eurjchem-1251	1	33	house	house	PROPN
eurjchem-1251	1	34	llc	llc	PROPN
eurjchem-1251	1	35	‐	‐	PUNCT
eurjchem-1251	1	36	all	all	DET
eurjchem-1251	1	37	rights	right	NOUN
eurjchem-1251	1	38	reserved	reserve	VERB
eurjchem-1251	1	39	‐	‐	NOUN
eurjchem-1251	1	40	printed	print	VERB
eurjchem-1251	1	41	in	in	ADP
eurjchem-1251	1	42	the	the	DET
eurjchem-1251	1	43	usa	usa	PROPN
eurjchem-1251	1	44	http://dx.doi.org/10.5155/eurjchem.6.2.211‐218.1251	http://dx.doi.org/10.5155/eurjchem.6.2.211‐218.1251	PROPN
eurjchem-1251	1	45	european	european	PROPN
eurjchem-1251	1	46	journal	journal	PROPN
eurjchem-1251	1	47	of	of	ADP
eurjchem-1251	1	48	chemistry	chemistry	PROPN
eurjchem-1251	1	49	journal	journal	PROPN
eurjchem-1251	1	50	webpage	webpage	NOUN
eurjchem-1251	1	51	:	:	PUNCT
eurjchem-1251	1	52	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1251	1	53	pyridazine	pyridazine	PROPN
eurjchem-1251	1	54	and	and	CCONJ
eurjchem-1251	1	55	its	its	PRON
eurjchem-1251	1	56	related	related	ADJ
eurjchem-1251	1	57	compounds	compound	NOUN
eurjchem-1251	1	58	:	:	PUNCT
eurjchem-1251	1	59	part	part	NOUN
eurjchem-1251	1	60	32	32	NUM
eurjchem-1251	1	61	.	.	PUNCT
eurjchem-1251	2	1	synthesis	synthesis	NOUN
eurjchem-1251	2	2	and	and	CCONJ
eurjchem-1251	2	3	antimicrobial	antimicrobial	ADJ
eurjchem-1251	2	4	evaluation	evaluation	NOUN
eurjchem-1251	2	5	of	of	ADP
eurjchem-1251	2	6	some	some	DET
eurjchem-1251	2	7	3‐substituted	3‐substituted	NUM
eurjchem-1251	2	8	amino‐4,5,6‐triphenylpyridazine	amino‐4,5,6‐triphenylpyridazine	PROPN
eurjchem-1251	2	9	derivatives	derivative	NOUN
eurjchem-1251	2	10	ali	ali	PROPN
eurjchem-1251	2	11	abdel	abdel	PROPN
eurjchem-1251	2	12	hamid	hamid	PROPN
eurjchem-1251	2	13	deeb	deeb	PROPN
eurjchem-1251	2	14	1	1	NUM
eurjchem-1251	2	15	,	,	PUNCT
eurjchem-1251	2	16	*	*	PUNCT
eurjchem-1251	2	17	,	,	PUNCT
eurjchem-1251	2	18	fatma	fatma	PROPN
eurjchem-1251	2	19	abdel	abdel	PROPN
eurjchem-1251	2	20	rahman	rahman	PROPN
eurjchem-1251	2	21	el‐mariah	el‐mariah	PROPN
eurjchem-1251	2	22	2	2	NUM
eurjchem-1251	2	23	and	and	CCONJ
eurjchem-1251	2	24	heba	heba	PROPN
eurjchem-1251	2	25	kamal	kamal	PROPN
eurjchem-1251	2	26	abd	abd	PROPN
eurjchem-1251	2	27	el‐mawgoud	el‐mawgoud	ADJ
eurjchem-1251	2	28	2	2	NUM
eurjchem-1251	2	29	1	1	NUM
eurjchem-1251	2	30	department	department	NOUN
eurjchem-1251	2	31	of	of	ADP
eurjchem-1251	2	32	chemistry	chemistry	NOUN
eurjchem-1251	2	33	,	,	PUNCT
eurjchem-1251	2	34	faculty	faculty	NOUN
eurjchem-1251	2	35	of	of	ADP
eurjchem-1251	2	36	science	science	NOUN
eurjchem-1251	2	37	,	,	PUNCT
eurjchem-1251	2	38	zagazig	zagazig	PROPN
eurjchem-1251	2	39	university	university	PROPN
eurjchem-1251	2	40	,	,	PUNCT
eurjchem-1251	2	41	zagazig	zagazig	PROPN
eurjchem-1251	2	42	,	,	PUNCT
eurjchem-1251	2	43	44519	44519	NUM
eurjchem-1251	2	44	,	,	PUNCT
eurjchem-1251	2	45	egypt	egypt	PROPN
eurjchem-1251	2	46	2	2	NUM
eurjchem-1251	2	47	department	department	NOUN
eurjchem-1251	2	48	of	of	ADP
eurjchem-1251	2	49	chemistry	chemistry	NOUN
eurjchem-1251	2	50	,	,	PUNCT
eurjchem-1251	2	51	college	college	NOUN
eurjchem-1251	2	52	of	of	ADP
eurjchem-1251	2	53	women	woman	NOUN
eurjchem-1251	2	54	for	for	ADP
eurjchem-1251	2	55	arts	art	NOUN
eurjchem-1251	2	56	,	,	PUNCT
eurjchem-1251	2	57	science	science	NOUN
eurjchem-1251	2	58	and	and	CCONJ
eurjchem-1251	2	59	education	education	NOUN
eurjchem-1251	2	60	,	,	PUNCT
eurjchem-1251	2	61	ain	ain	PROPN
eurjchem-1251	2	62	shams	shams	PROPN
eurjchem-1251	2	63	university	university	PROPN
eurjchem-1251	2	64	,	,	PUNCT
eurjchem-1251	2	65	cairo	cairo	PROPN
eurjchem-1251	2	66	,	,	PUNCT
eurjchem-1251	2	67	11753	11753	NUM
eurjchem-1251	2	68	,	,	PUNCT
eurjchem-1251	2	69	egypt	egypt	PROPN
eurjchem-1251	2	70	*	*	PUNCT
eurjchem-1251	2	71	corresponding	correspond	VERB
eurjchem-1251	2	72	author	author	NOUN
eurjchem-1251	2	73	at	at	ADP
eurjchem-1251	2	74	:	:	PUNCT
eurjchem-1251	2	75	department	department	NOUN
eurjchem-1251	2	76	of	of	ADP
eurjchem-1251	2	77	chemistry	chemistry	NOUN
eurjchem-1251	2	78	,	,	PUNCT
eurjchem-1251	2	79	faculty	faculty	NOUN
eurjchem-1251	2	80	of	of	ADP
eurjchem-1251	2	81	science	science	NOUN
eurjchem-1251	2	82	,	,	PUNCT
eurjchem-1251	2	83	zagazig	zagazig	PROPN
eurjchem-1251	2	84	university	university	PROPN
eurjchem-1251	2	85	,	,	PUNCT
eurjchem-1251	2	86	zagazig	zagazig	PROPN
eurjchem-1251	2	87	,	,	PUNCT
eurjchem-1251	2	88	44519	44519	NUM
eurjchem-1251	2	89	,	,	PUNCT
eurjchem-1251	2	90	egypt	egypt	PROPN
eurjchem-1251	2	91	.	.	PUNCT
eurjchem-1251	3	1	tel	tel	PROPN
eurjchem-1251	3	2	.	.	PUNCT
eurjchem-1251	3	3	:	:	PUNCT
eurjchem-1251	4	1	+20.55.2303252	+20.55.2303252	NUM
eurjchem-1251	4	2	.	.	PUNCT
eurjchem-1251	4	3	fax	fax	NOUN
eurjchem-1251	4	4	:	:	PUNCT
eurjchem-1251	4	5	+20.55.2308213	+20.55.2308213	NUM
eurjchem-1251	4	6	.	.	PUNCT
eurjchem-1251	4	7	e‐mail	e‐mail	PUNCT
eurjchem-1251	4	8	address	address	NOUN
eurjchem-1251	4	9	:	:	PUNCT
eurjchem-1251	4	10	dralideeb@hotmail.com	dralideeb@hotmail.com	PROPN
eurjchem-1251	4	11	(	(	PUNCT
eurjchem-1251	4	12	a.a	a.a	PROPN
eurjchem-1251	4	13	.	.	PROPN
eurjchem-1251	4	14	deeb	deeb	PROPN
eurjchem-1251	4	15	)	)	PUNCT
eurjchem-1251	4	16	.	.	PUNCT
eurjchem-1251	5	1	article	article	NOUN
eurjchem-1251	5	2	information	information	PROPN
eurjchem-1251	5	3	abstract	abstract	ADJ
eurjchem-1251	5	4	doi	doi	NOUN
eurjchem-1251	5	5	:	:	PUNCT
eurjchem-1251	5	6	10.5155	10.5155	NUM
eurjchem-1251	5	7	/	/	SYM
eurjchem-1251	5	8	eurjchem.6.2.211‐218.1251	eurjchem.6.2.211‐218.1251	PRON
eurjchem-1251	5	9	received	receive	VERB
eurjchem-1251	5	10	:	:	PUNCT
eurjchem-1251	5	11	04	04	NUM
eurjchem-1251	5	12	february	february	NOUN
eurjchem-1251	5	13	2015	2015	NUM
eurjchem-1251	5	14	received	receive	VERB
eurjchem-1251	5	15	in	in	ADP
eurjchem-1251	5	16	revised	revise	VERB
eurjchem-1251	5	17	form	form	NOUN
eurjchem-1251	5	18	:	:	PUNCT
eurjchem-1251	5	19	25	25	NUM
eurjchem-1251	5	20	april	april	PROPN
eurjchem-1251	5	21	2015	2015	NUM
eurjchem-1251	5	22	accepted	accept	VERB
eurjchem-1251	5	23	:	:	PUNCT
eurjchem-1251	5	24	01	01	NUM
eurjchem-1251	5	25	may	may	AUX
eurjchem-1251	5	26	2015	2015	NUM
eurjchem-1251	5	27	published	publish	VERB
eurjchem-1251	5	28	online	online	ADV
eurjchem-1251	5	29	:	:	PUNCT
eurjchem-1251	5	30	30	30	NUM
eurjchem-1251	5	31	june	june	PROPN
eurjchem-1251	5	32	2015	2015	NUM
eurjchem-1251	5	33	printed	print	VERB
eurjchem-1251	5	34	:	:	PUNCT
eurjchem-1251	5	35	30	30	NUM
eurjchem-1251	5	36	june	june	PROPN
eurjchem-1251	5	37	2015	2015	NUM
eurjchem-1251	5	38	3‐amino‐4,5,6‐triphenylpyridazine	3‐amino‐4,5,6‐triphenylpyridazine	NUM
eurjchem-1251	5	39	was	be	AUX
eurjchem-1251	5	40	subjected	subject	VERB
eurjchem-1251	5	41	to	to	ADP
eurjchem-1251	5	42	some	some	DET
eurjchem-1251	5	43	selected	select	VERB
eurjchem-1251	5	44	reactions	reaction	NOUN
eurjchem-1251	5	45	with	with	ADP
eurjchem-1251	5	46	nitrous	nitrous	ADJ
eurjchem-1251	5	47	acid	acid	NOUN
eurjchem-1251	5	48	,	,	PUNCT
eurjchem-1251	5	49	formic	formic	ADJ
eurjchem-1251	5	50	acid	acid	NOUN
eurjchem-1251	5	51	/	/	SYM
eurjchem-1251	5	52	dimethylformamide	dimethylformamide	NOUN
eurjchem-1251	5	53	,	,	PUNCT
eurjchem-1251	5	54	acetic	acetic	ADJ
eurjchem-1251	5	55	anhydride	anhydride	NOUN
eurjchem-1251	5	56	,	,	PUNCT
eurjchem-1251	5	57	benzoyl	benzoyl	NOUN
eurjchem-1251	5	58	chloride	chloride	NOUN
eurjchem-1251	5	59	,	,	PUNCT
eurjchem-1251	5	60	chloroacetyl	chloroacetyl	NOUN
eurjchem-1251	5	61	chloride	chloride	NOUN
eurjchem-1251	5	62	,	,	PUNCT
eurjchem-1251	5	63	acetaldehyde	acetaldehyde	NOUN
eurjchem-1251	5	64	,	,	PUNCT
eurjchem-1251	5	65	diethyl	diethyl	NOUN
eurjchem-1251	5	66	malonate	malonate	NOUN
eurjchem-1251	5	67	,	,	PUNCT
eurjchem-1251	5	68	malonic	malonic	ADJ
eurjchem-1251	5	69	acid	acid	NOUN
eurjchem-1251	5	70	/	/	SYM
eurjchem-1251	5	71	phosphoryl	phosphoryl	NOUN
eurjchem-1251	5	72	chloride	chloride	NOUN
eurjchem-1251	5	73	,	,	PUNCT
eurjchem-1251	5	74	diethyl	diethyl	NOUN
eurjchem-1251	5	75	oxalate	oxalate	NOUN
eurjchem-1251	5	76	,	,	PUNCT
eurjchem-1251	5	77	ethyl	ethyl	PROPN
eurjchem-1251	5	78	cyanoacetate	cyanoacetate	PROPN
eurjchem-1251	5	79	,	,	PUNCT
eurjchem-1251	5	80	ethyl	ethyl	PROPN
eurjchem-1251	5	81	acetoacetate	acetoacetate	NOUN
eurjchem-1251	5	82	,	,	PUNCT
eurjchem-1251	5	83	and	and	CCONJ
eurjchem-1251	5	84	ethyl	ethyl	PROPN
eurjchem-1251	5	85	benzoylacetate	benzoylacetate	NOUN
eurjchem-1251	5	86	to	to	PART
eurjchem-1251	5	87	give	give	VERB
eurjchem-1251	5	88	new	new	ADJ
eurjchem-1251	5	89	3‐substituted	3‐substitute	VERB
eurjchem-1251	5	90	aminopyridazine	aminopyridazine	NOUN
eurjchem-1251	5	91	derivatives	derivative	NOUN
eurjchem-1251	5	92	.	.	PUNCT
eurjchem-1251	6	1	a	a	DET
eurjchem-1251	6	2	few	few	ADJ
eurjchem-1251	6	3	sulfonamide	sulfonamide	ADJ
eurjchem-1251	6	4	derivatives	derivative	NOUN
eurjchem-1251	6	5	(	(	PUNCT
eurjchem-1251	6	6	new	new	ADJ
eurjchem-1251	6	7	)	)	PUNCT
eurjchem-1251	6	8	were	be	AUX
eurjchem-1251	6	9	also	also	ADV
eurjchem-1251	6	10	prepared	prepare	VERB
eurjchem-1251	6	11	.	.	PUNCT
eurjchem-1251	7	1	the	the	DET
eurjchem-1251	7	2	structures	structure	NOUN
eurjchem-1251	7	3	of	of	ADP
eurjchem-1251	7	4	the	the	DET
eurjchem-1251	7	5	synthesized	synthesize	VERB
eurjchem-1251	7	6	compounds	compound	NOUN
eurjchem-1251	7	7	were	be	AUX
eurjchem-1251	7	8	proved	prove	VERB
eurjchem-1251	7	9	by	by	ADP
eurjchem-1251	7	10	their	their	PRON
eurjchem-1251	7	11	infrared	infrared	NOUN
eurjchem-1251	7	12	,	,	PUNCT
eurjchem-1251	7	13	mass	mass	PROPN
eurjchem-1251	7	14	spectra	spectra	PROPN
eurjchem-1251	7	15	,	,	PUNCT
eurjchem-1251	7	16	1h	1h	NUM
eurjchem-1251	7	17	nmr	nmr	NOUN
eurjchem-1251	7	18	,	,	PUNCT
eurjchem-1251	7	19	and	and	CCONJ
eurjchem-1251	7	20	elemental	elemental	ADJ
eurjchem-1251	7	21	analysis	analysis	NOUN
eurjchem-1251	7	22	.	.	PUNCT
eurjchem-1251	8	1	the	the	DET
eurjchem-1251	8	2	antimicrobial	antimicrobial	ADJ
eurjchem-1251	8	3	activity	activity	NOUN
eurjchem-1251	8	4	of	of	ADP
eurjchem-1251	8	5	the	the	DET
eurjchem-1251	8	6	compounds	compound	NOUN
eurjchem-1251	8	7	obtained	obtain	VERB
eurjchem-1251	8	8	was	be	AUX
eurjchem-1251	8	9	examined	examine	VERB
eurjchem-1251	8	10	against	against	ADP
eurjchem-1251	8	11	some	some	DET
eurjchem-1251	8	12	selected	select	VERB
eurjchem-1251	8	13	microorganisms	microorganism	NOUN
eurjchem-1251	8	14	.	.	PUNCT
eurjchem-1251	9	1	keywords	keyword	VERB
eurjchem-1251	9	2	3‐aminopyridazin	3‐aminopyridazin	NUM
eurjchem-1251	9	3	anti‐microbial	anti‐microbial	ADJ
eurjchem-1251	9	4	activity	activity	NOUN
eurjchem-1251	9	5	benzil	benzil	NOUN
eurjchem-1251	9	6	monohydrazone	monohydrazone	NOUN
eurjchem-1251	9	7	pyridazine	pyridazine	NOUN
eurjchem-1251	9	8	sulfonamides	sulfonamide	VERB
eurjchem-1251	9	9	pyrimido[1,2‐b]pyridazines	pyrimido[1,2‐b]pyridazine	NOUN
eurjchem-1251	9	10	3‐substituted	3‐substituted	NUM
eurjchem-1251	9	11	aminopyridazine	aminopyridazine	NOUN
eurjchem-1251	9	12	cite	cite	VERB
eurjchem-1251	9	13	this	this	PRON
eurjchem-1251	9	14	:	:	PUNCT
eurjchem-1251	9	15	eur	eur	PROPN
eurjchem-1251	9	16	.	.	PUNCT
eurjchem-1251	10	1	j.	j.	PROPN
eurjchem-1251	10	2	chem	chem	PROPN
eurjchem-1251	10	3	.	.	PUNCT
eurjchem-1251	11	1	2015	2015	NUM
eurjchem-1251	11	2	,	,	PUNCT
eurjchem-1251	11	3	6(2	6(2	NUM
eurjchem-1251	11	4	)	)	PUNCT
eurjchem-1251	11	5	,	,	PUNCT
eurjchem-1251	11	6	211‐218	211‐218	NUM
eurjchem-1251	11	7	1	1	NUM
eurjchem-1251	11	8	.	.	PUNCT
eurjchem-1251	12	1	introduction	introduction	NOUN
eurjchem-1251	12	2	the	the	DET
eurjchem-1251	12	3	pyridazine	pyridazine	PROPN
eurjchem-1251	12	4	nucleus	nucleus	PROPN
eurjchem-1251	12	5	is	be	AUX
eurjchem-1251	12	6	a	a	DET
eurjchem-1251	12	7	very	very	ADV
eurjchem-1251	12	8	common	common	ADJ
eurjchem-1251	12	9	component	component	NOUN
eurjchem-1251	12	10	in	in	ADP
eurjchem-1251	12	11	many	many	ADJ
eurjchem-1251	12	12	compounds	compound	NOUN
eurjchem-1251	12	13	of	of	ADP
eurjchem-1251	12	14	biological	biological	ADJ
eurjchem-1251	12	15	interest	interest	NOUN
eurjchem-1251	12	16	manifested	manifest	VERB
eurjchem-1251	12	17	in	in	ADP
eurjchem-1251	12	18	several	several	ADJ
eurjchem-1251	12	19	fields	field	NOUN
eurjchem-1251	12	20	of	of	ADP
eurjchem-1251	12	21	medicinal	medicinal	ADJ
eurjchem-1251	12	22	chemistry	chemistry	NOUN
eurjchem-1251	12	23	,	,	PUNCT
eurjchem-1251	12	24	such	such	ADJ
eurjchem-1251	12	25	as	as	ADP
eurjchem-1251	12	26	phosphodiesterase	phosphodiesterase	NOUN
eurjchem-1251	12	27	type	type	NOUN
eurjchem-1251	12	28	4	4	NUM
eurjchem-1251	12	29	inhibitors	inhibitor	NOUN
eurjchem-1251	12	30	for	for	ADP
eurjchem-1251	12	31	inflammatory	inflammatory	ADJ
eurjchem-1251	12	32	diseases	disease	NOUN
eurjchem-1251	13	1	[	[	X
eurjchem-1251	13	2	1	1	NUM
eurjchem-1251	13	3	]	]	PUNCT
eurjchem-1251	13	4	,	,	PUNCT
eurjchem-1251	13	5	as	as	SCONJ
eurjchem-1251	13	6	endothelin‐a	endothelin‐a	NOUN
eurjchem-1251	13	7	receptor	receptor	NOUN
eurjchem-1251	13	8	antagonists	antagonist	NOUN
eurjchem-1251	14	1	[	[	X
eurjchem-1251	14	2	2	2	NUM
eurjchem-1251	14	3	]	]	PUNCT
eurjchem-1251	14	4	,	,	PUNCT
eurjchem-1251	14	5	in	in	ADP
eurjchem-1251	14	6	the	the	DET
eurjchem-1251	14	7	development	development	NOUN
eurjchem-1251	14	8	of	of	ADP
eurjchem-1251	14	9	active	active	ADJ
eurjchem-1251	14	10	compounds	compound	NOUN
eurjchem-1251	14	11	toward	toward	ADP
eurjchem-1251	14	12	α1	α1	PROPN
eurjchem-1251	14	13	and	and	CCONJ
eurjchem-1251	14	14	α2	α2	ADJ
eurjchem-1251	14	15	adrenoceptors	adrenoceptor	NOUN
eurjchem-1251	15	1	[	[	X
eurjchem-1251	15	2	3	3	NUM
eurjchem-1251	15	3	]	]	PUNCT
eurjchem-1251	15	4	,	,	PUNCT
eurjchem-1251	15	5	as	as	SCONJ
eurjchem-1251	15	6	central	central	ADJ
eurjchem-1251	15	7	analgesics	analgesic	NOUN
eurjchem-1251	15	8	and	and	CCONJ
eurjchem-1251	15	9	aldose	aldose	PROPN
eurjchem-1251	15	10	reductose	reductose	VERB
eurjchem-1251	15	11	inhibitors	inhibitor	NOUN
eurjchem-1251	15	12	[	[	X
eurjchem-1251	15	13	4	4	NUM
eurjchem-1251	15	14	]	]	PUNCT
eurjchem-1251	15	15	.	.	PUNCT
eurjchem-1251	16	1	the	the	DET
eurjchem-1251	16	2	pyridazine	pyridazine	NOUN
eurjchem-1251	16	3	derivatives	derivative	NOUN
eurjchem-1251	16	4	are	be	AUX
eurjchem-1251	16	5	also	also	ADV
eurjchem-1251	16	6	used	use	VERB
eurjchem-1251	16	7	as	as	ADP
eurjchem-1251	16	8	analgesic	analgesic	ADJ
eurjchem-1251	16	9	[	[	X
eurjchem-1251	16	10	5	5	NUM
eurjchem-1251	16	11	]	]	PUNCT
eurjchem-1251	16	12	,	,	PUNCT
eurjchem-1251	16	13	antibacterial	antibacterial	ADJ
eurjchem-1251	16	14	[	[	X
eurjchem-1251	16	15	6	6	NUM
eurjchem-1251	16	16	]	]	PUNCT
eurjchem-1251	16	17	,	,	PUNCT
eurjchem-1251	16	18	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-1251	17	1	[	[	X
eurjchem-1251	17	2	7	7	NUM
eurjchem-1251	17	3	]	]	PUNCT
eurjchem-1251	17	4	,	,	PUNCT
eurjchem-1251	17	5	anti‐hypertensive	anti‐hypertensive	VERB
eurjchem-1251	18	1	[	[	X
eurjchem-1251	18	2	8	8	NUM
eurjchem-1251	18	3	]	]	PUNCT
eurjchem-1251	18	4	,	,	PUNCT
eurjchem-1251	18	5	antihistaminic	antihistaminic	NOUN
eurjchem-1251	18	6	[	[	X
eurjchem-1251	18	7	9	9	NUM
eurjchem-1251	18	8	]	]	PUNCT
eurjchem-1251	18	9	,	,	PUNCT
eurjchem-1251	18	10	antinociceptive	antinociceptive	ADJ
eurjchem-1251	18	11	agents	agent	NOUN
eurjchem-1251	19	1	[	[	X
eurjchem-1251	19	2	10	10	NUM
eurjchem-1251	19	3	]	]	PUNCT
eurjchem-1251	19	4	,	,	PUNCT
eurjchem-1251	19	5	as	as	ADV
eurjchem-1251	19	6	well	well	ADV
eurjchem-1251	19	7	as	as	ADP
eurjchem-1251	19	8	platelet	platelet	NOUN
eurjchem-1251	19	9	aggregation	aggregation	NOUN
eurjchem-1251	19	10	inhibitors	inhibitor	NOUN
eurjchem-1251	20	1	[	[	X
eurjchem-1251	20	2	11	11	NUM
eurjchem-1251	20	3	]	]	PUNCT
eurjchem-1251	20	4	.	.	PUNCT
eurjchem-1251	21	1	they	they	PRON
eurjchem-1251	21	2	have	have	VERB
eurjchem-1251	21	3	a	a	DET
eurjchem-1251	21	4	rapid	rapid	ADJ
eurjchem-1251	21	5	systemic	systemic	ADJ
eurjchem-1251	21	6	effect	effect	NOUN
eurjchem-1251	21	7	on	on	ADP
eurjchem-1251	21	8	the	the	DET
eurjchem-1251	21	9	plants	plant	NOUN
eurjchem-1251	21	10	and	and	CCONJ
eurjchem-1251	21	11	are	be	AUX
eurjchem-1251	21	12	active	active	ADJ
eurjchem-1251	21	13	at	at	ADP
eurjchem-1251	21	14	very	very	ADV
eurjchem-1251	21	15	low	low	ADJ
eurjchem-1251	21	16	concentration	concentration	NOUN
eurjchem-1251	21	17	.	.	PUNCT
eurjchem-1251	22	1	some	some	PRON
eurjchem-1251	22	2	of	of	ADP
eurjchem-1251	22	3	the	the	DET
eurjchem-1251	22	4	investigated	investigate	VERB
eurjchem-1251	22	5	pyridazine	pyridazine	NOUN
eurjchem-1251	22	6	derivatives	derivative	NOUN
eurjchem-1251	22	7	have	have	VERB
eurjchem-1251	22	8	chemical	chemical	NOUN
eurjchem-1251	22	9	structures	structure	NOUN
eurjchem-1251	22	10	related	relate	VERB
eurjchem-1251	22	11	to	to	ADP
eurjchem-1251	22	12	those	those	PRON
eurjchem-1251	22	13	of	of	ADP
eurjchem-1251	22	14	the	the	DET
eurjchem-1251	22	15	phytohormones	phytohormone	NOUN
eurjchem-1251	22	16	[	[	X
eurjchem-1251	22	17	12	12	NUM
eurjchem-1251	22	18	]	]	PUNCT
eurjchem-1251	22	19	.	.	PUNCT
eurjchem-1251	23	1	in	in	ADP
eurjchem-1251	23	2	addition	addition	NOUN
eurjchem-1251	23	3	,	,	PUNCT
eurjchem-1251	23	4	similar	similar	ADJ
eurjchem-1251	23	5	chemical	chemical	NOUN
eurjchem-1251	23	6	structures	structure	NOUN
eurjchem-1251	23	7	occur	occur	VERB
eurjchem-1251	23	8	in	in	ADP
eurjchem-1251	23	9	living	living	NOUN
eurjchem-1251	23	10	cells	cell	NOUN
eurjchem-1251	23	11	,	,	PUNCT
eurjchem-1251	23	12	being	be	AUX
eurjchem-1251	23	13	involved	involve	VERB
eurjchem-1251	23	14	in	in	ADP
eurjchem-1251	23	15	various	various	ADJ
eurjchem-1251	23	16	biochemical	biochemical	ADJ
eurjchem-1251	23	17	reaction	reaction	NOUN
eurjchem-1251	23	18	pathways	pathway	NOUN
eurjchem-1251	23	19	.	.	PUNCT
eurjchem-1251	24	1	some	some	DET
eurjchem-1251	24	2	new	new	ADJ
eurjchem-1251	24	3	synthesized	synthesize	VERB
eurjchem-1251	24	4	pyridazine	pyridazine	NOUN
eurjchem-1251	24	5	derivatives	derivative	NOUN
eurjchem-1251	24	6	were	be	AUX
eurjchem-1251	24	7	used	use	VERB
eurjchem-1251	24	8	in	in	ADP
eurjchem-1251	24	9	many	many	ADJ
eurjchem-1251	24	10	research	research	NOUN
eurjchem-1251	24	11	fields	field	NOUN
eurjchem-1251	24	12	due	due	ADP
eurjchem-1251	24	13	to	to	ADP
eurjchem-1251	24	14	their	their	PRON
eurjchem-1251	24	15	structure	structure	NOUN
eurjchem-1251	24	16	,	,	PUNCT
eurjchem-1251	24	17	stability	stability	NOUN
eurjchem-1251	24	18	,	,	PUNCT
eurjchem-1251	24	19	reactivity	reactivity	NOUN
eurjchem-1251	24	20	and	and	CCONJ
eurjchem-1251	24	21	their	their	PRON
eurjchem-1251	24	22	tendency	tendency	NOUN
eurjchem-1251	24	23	to	to	PART
eurjchem-1251	24	24	form	form	VERB
eurjchem-1251	24	25	stable	stable	ADJ
eurjchem-1251	24	26	derivatives	derivative	NOUN
eurjchem-1251	24	27	with	with	ADP
eurjchem-1251	24	28	important	important	ADJ
eurjchem-1251	24	29	biological	biological	ADJ
eurjchem-1251	24	30	properties	property	NOUN
eurjchem-1251	24	31	.	.	PUNCT
eurjchem-1251	25	1	on	on	ADP
eurjchem-1251	25	2	the	the	DET
eurjchem-1251	25	3	other	other	ADJ
eurjchem-1251	25	4	hand	hand	NOUN
eurjchem-1251	25	5	,	,	PUNCT
eurjchem-1251	25	6	as	as	ADP
eurjchem-1251	25	7	a	a	DET
eurjchem-1251	25	8	rule	rule	NOUN
eurjchem-1251	25	9	,	,	PUNCT
eurjchem-1251	25	10	a	a	DET
eurjchem-1251	25	11	cytotoxic	cytotoxic	ADJ
eurjchem-1251	25	12	effect	effect	NOUN
eurjchem-1251	25	13	of	of	ADP
eurjchem-1251	25	14	higher	high	ADJ
eurjchem-1251	25	15	concentrated	concentrated	ADJ
eurjchem-1251	25	16	compounds	compound	NOUN
eurjchem-1251	25	17	is	be	AUX
eurjchem-1251	25	18	correlated	correlate	VERB
eurjchem-1251	25	19	with	with	ADP
eurjchem-1251	25	20	their	their	PRON
eurjchem-1251	25	21	stimulation	stimulation	NOUN
eurjchem-1251	25	22	effect	effect	NOUN
eurjchem-1251	25	23	at	at	ADP
eurjchem-1251	25	24	lower	low	ADJ
eurjchem-1251	25	25	concentrations	concentration	NOUN
eurjchem-1251	25	26	[	[	X
eurjchem-1251	25	27	13	13	NUM
eurjchem-1251	25	28	]	]	PUNCT
eurjchem-1251	25	29	.	.	PUNCT
eurjchem-1251	26	1	thus	thus	ADV
eurjchem-1251	26	2	,	,	PUNCT
eurjchem-1251	26	3	due	due	ADP
eurjchem-1251	26	4	to	to	ADP
eurjchem-1251	26	5	this	this	DET
eurjchem-1251	26	6	wide	wide	ADJ
eurjchem-1251	26	7	use	use	NOUN
eurjchem-1251	26	8	of	of	ADP
eurjchem-1251	26	9	pyridazine	pyridazine	NOUN
eurjchem-1251	26	10	based	base	VERB
eurjchem-1251	26	11	structures	structure	NOUN
eurjchem-1251	26	12	,	,	PUNCT
eurjchem-1251	26	13	great	great	ADJ
eurjchem-1251	26	14	attention	attention	NOUN
eurjchem-1251	26	15	was	be	AUX
eurjchem-1251	26	16	paid	pay	VERB
eurjchem-1251	26	17	to	to	ADP
eurjchem-1251	26	18	the	the	DET
eurjchem-1251	26	19	development	development	NOUN
eurjchem-1251	26	20	of	of	ADP
eurjchem-1251	26	21	different	different	ADJ
eurjchem-1251	26	22	methods	method	NOUN
eurjchem-1251	26	23	for	for	ADP
eurjchem-1251	26	24	the	the	DET
eurjchem-1251	26	25	preparation	preparation	NOUN
eurjchem-1251	26	26	of	of	ADP
eurjchem-1251	26	27	pyridazine	pyridazine	NOUN
eurjchem-1251	26	28	and	and	CCONJ
eurjchem-1251	26	29	its	its	PRON
eurjchem-1251	26	30	functionalized	functionalized	ADJ
eurjchem-1251	26	31	derivatives	derivative	NOUN
eurjchem-1251	26	32	.	.	PUNCT
eurjchem-1251	27	1	2	2	X
eurjchem-1251	27	2	.	.	X
eurjchem-1251	27	3	experimental	experimental	ADJ
eurjchem-1251	27	4	2.1	2.1	NUM
eurjchem-1251	27	5	.	.	PUNCT
eurjchem-1251	27	6	instrumentation	instrumentation	NOUN
eurjchem-1251	27	7	all	all	DET
eurjchem-1251	27	8	melting	melt	VERB
eurjchem-1251	27	9	points	point	NOUN
eurjchem-1251	27	10	were	be	AUX
eurjchem-1251	27	11	determined	determine	VERB
eurjchem-1251	27	12	in	in	ADP
eurjchem-1251	27	13	open	open	ADJ
eurjchem-1251	27	14	glass	glass	NOUN
eurjchem-1251	27	15	capillaries	capillary	NOUN
eurjchem-1251	27	16	and	and	CCONJ
eurjchem-1251	27	17	are	be	AUX
eurjchem-1251	27	18	uncorrected	uncorrecte	VERB
eurjchem-1251	27	19	.	.	PUNCT
eurjchem-1251	28	1	elemental	elemental	ADJ
eurjchem-1251	28	2	analyses	analysis	NOUN
eurjchem-1251	28	3	were	be	AUX
eurjchem-1251	28	4	carried	carry	VERB
eurjchem-1251	28	5	out	out	ADP
eurjchem-1251	28	6	in	in	ADP
eurjchem-1251	28	7	the	the	DET
eurjchem-1251	28	8	micro	micro	ADJ
eurjchem-1251	28	9	analytical	analytical	ADJ
eurjchem-1251	28	10	laboratory	laboratory	NOUN
eurjchem-1251	28	11	of	of	ADP
eurjchem-1251	28	12	the	the	DET
eurjchem-1251	28	13	faculty	faculty	NOUN
eurjchem-1251	28	14	of	of	ADP
eurjchem-1251	28	15	science	science	NOUN
eurjchem-1251	28	16	,	,	PUNCT
eurjchem-1251	28	17	cairo	cairo	PROPN
eurjchem-1251	28	18	university	university	PROPN
eurjchem-1251	28	19	.	.	PUNCT
eurjchem-1251	29	1	the	the	DET
eurjchem-1251	29	2	ir	ir	PROPN
eurjchem-1251	29	3	spectra	spectra	NOUN
eurjchem-1251	29	4	of	of	ADP
eurjchem-1251	29	5	compounds	compound	NOUN
eurjchem-1251	29	6	were	be	AUX
eurjchem-1251	29	7	recorded	record	VERB
eurjchem-1251	29	8	on	on	ADP
eurjchem-1251	29	9	a	a	DET
eurjchem-1251	29	10	nicolet	nicolet	PROPN
eurjchem-1251	29	11	6700	6700	NUM
eurjchem-1251	29	12	ft‐ir	ft‐ir	NOUN
eurjchem-1251	29	13	(	(	PUNCT
eurjchem-1251	29	14	thermo	thermo	NOUN
eurjchem-1251	29	15	scientific	scientific	NOUN
eurjchem-1251	29	16	)	)	PUNCT
eurjchem-1251	29	17	as	as	SCONJ
eurjchem-1251	29	18	potassium	potassium	NOUN
eurjchem-1251	29	19	bromide	bromide	NOUN
eurjchem-1251	29	20	pellets	pellet	NOUN
eurjchem-1251	29	21	and	and	CCONJ
eurjchem-1251	29	22	frequencies	frequency	NOUN
eurjchem-1251	29	23	are	be	AUX
eurjchem-1251	29	24	reported	report	VERB
eurjchem-1251	29	25	in	in	ADP
eurjchem-1251	29	26	cm‐1	cm‐1	PROPN
eurjchem-1251	29	27	.	.	PUNCT
eurjchem-1251	30	1	the	the	DET
eurjchem-1251	30	2	mass	mass	ADJ
eurjchem-1251	30	3	spectra	spectra	NOUN
eurjchem-1251	30	4	were	be	AUX
eurjchem-1251	30	5	recorded	record	VERB
eurjchem-1251	30	6	on	on	ADP
eurjchem-1251	30	7	a	a	DET
eurjchem-1251	30	8	gc‐ms	gc‐ms	NOUN
eurjchem-1251	30	9	model	model	NOUN
eurjchem-1251	30	10	shimadzu	shimadzu	NOUN
eurjchem-1251	30	11	qp‐2010	qp‐2010	PROPN
eurjchem-1251	30	12	plus	plus	CCONJ
eurjchem-1251	30	13	ei	ei	ADP
eurjchem-1251	30	14	70	70	NUM
eurjchem-1251	30	15	ev	ev	NOUN
eurjchem-1251	30	16	.	.	PUNCT
eurjchem-1251	31	1	the	the	DET
eurjchem-1251	31	2	1h	1h	NUM
eurjchem-1251	31	3	nmr	nmr	NOUN
eurjchem-1251	31	4	spectra	spectra	NOUN
eurjchem-1251	31	5	were	be	AUX
eurjchem-1251	31	6	recorded	record	VERB
eurjchem-1251	31	7	on	on	ADP
eurjchem-1251	31	8	a	a	DET
eurjchem-1251	31	9	varian	varian	NOUN
eurjchem-1251	31	10	gemini‐	gemini‐	PROPN
eurjchem-1251	31	11	300	300	NUM
eurjchem-1251	31	12	mhz	mhz	ADJ
eurjchem-1251	31	13	nmr	nmr	NOUN
eurjchem-1251	31	14	spectrometer	spectrometer	NOUN
eurjchem-1251	31	15	and	and	CCONJ
eurjchem-1251	31	16	chemical	chemical	NOUN
eurjchem-1251	31	17	shifts	shift	NOUN
eurjchem-1251	31	18	δ	δ	PRON
eurjchem-1251	31	19	are	be	AUX
eurjchem-1251	31	20	in	in	ADP
eurjchem-1251	31	21	ppm	ppm	NOUN
eurjchem-1251	31	22	relative	relative	ADJ
eurjchem-1251	31	23	to	to	ADP
eurjchem-1251	31	24	internal	internal	ADJ
eurjchem-1251	31	25	tms	tms	PROPN
eurjchem-1251	31	26	.	.	PUNCT
eurjchem-1251	32	1	reactions	reaction	NOUN
eurjchem-1251	32	2	were	be	AUX
eurjchem-1251	32	3	routinely	routinely	ADV
eurjchem-1251	32	4	followed	follow	VERB
eurjchem-1251	32	5	by	by	ADP
eurjchem-1251	32	6	thin	thin	ADJ
eurjchem-1251	32	7	layer	layer	NOUN
eurjchem-1251	32	8	chromatography	chromatography	NOUN
eurjchem-1251	32	9	(	(	PUNCT
eurjchem-1251	32	10	tlc	tlc	NOUN
eurjchem-1251	32	11	)	)	PUNCT
eurjchem-1251	32	12	on	on	ADP
eurjchem-1251	32	13	silica	silica	NOUN
eurjchem-1251	32	14	gel	gel	NOUN
eurjchem-1251	32	15	;	;	PUNCT
eurjchem-1251	32	16	f254	f254	NUM
eurjchem-1251	32	17	aluminum	aluminum	NOUN
eurjchem-1251	32	18	sheets	sheet	NOUN
eurjchem-1251	32	19	(	(	PUNCT
eurjchem-1251	32	20	merck	merck	NOUN
eurjchem-1251	32	21	)	)	PUNCT
eurjchem-1251	32	22	.	.	PUNCT
eurjchem-1251	33	1	the	the	DET
eurjchem-1251	33	2	spots	spot	NOUN
eurjchem-1251	33	3	were	be	AUX
eurjchem-1251	33	4	detected	detect	VERB
eurjchem-1251	33	5	by	by	ADP
eurjchem-1251	33	6	uv	uv	NOUN
eurjchem-1251	33	7	irradiation	irradiation	NOUN
eurjchem-1251	33	8	at	at	ADP
eurjchem-1251	33	9	254‐365	254‐365	NUM
eurjchem-1251	33	10	nm	nm	NOUN
eurjchem-1251	33	11	.	.	PUNCT
eurjchem-1251	34	1	212	212	NUM
eurjchem-1251	34	2	deeb	deeb	PROPN
eurjchem-1251	34	3	et	et	PROPN
eurjchem-1251	34	4	al	al	PROPN
eurjchem-1251	34	5	.	.	PUNCT
eurjchem-1251	34	6	/	/	SYM
eurjchem-1251	34	7	european	european	PROPN
eurjchem-1251	34	8	journal	journal	PROPN
eurjchem-1251	34	9	of	of	ADP
eurjchem-1251	34	10	chemistry	chemistry	NOUN
eurjchem-1251	34	11	6	6	NUM
eurjchem-1251	34	12	(	(	PUNCT
eurjchem-1251	34	13	2	2	NUM
eurjchem-1251	34	14	)	)	PUNCT
eurjchem-1251	34	15	(	(	PUNCT
eurjchem-1251	34	16	2015	2015	NUM
eurjchem-1251	34	17	)	)	PUNCT
eurjchem-1251	34	18	211‐218	211‐218	NUM
eurjchem-1251	34	19	scheme	scheme	NOUN
eurjchem-1251	34	20	1	1	NUM
eurjchem-1251	34	21	2.2	2.2	NUM
eurjchem-1251	34	22	.	.	PUNCT
eurjchem-1251	35	1	synthesis	synthesis	NOUN
eurjchem-1251	35	2	2.2.1	2.2.1	NUM
eurjchem-1251	35	3	.	.	PUNCT
eurjchem-1251	35	4	synthesis	synthesis	NOUN
eurjchem-1251	35	5	of	of	ADP
eurjchem-1251	35	6	4,5,6‐triphenylpyridazin‐3(2h)‐one	4,5,6‐triphenylpyridazin‐3(2h)‐one	NUM
eurjchem-1251	35	7	(	(	PUNCT
eurjchem-1251	35	8	1	1	NUM
eurjchem-1251	35	9	)	)	PUNCT
eurjchem-1251	35	10	4,5,6‐triphenylpyridazin‐3(2h)‐one	4,5,6‐triphenylpyridazin‐3(2h)‐one	NOUN
eurjchem-1251	35	11	(	(	PUNCT
eurjchem-1251	35	12	1	1	NUM
eurjchem-1251	35	13	)	)	PUNCT
eurjchem-1251	35	14	was	be	AUX
eurjchem-1251	35	15	prepared	prepare	VERB
eurjchem-1251	35	16	according	accord	VERB
eurjchem-1251	35	17	to	to	ADP
eurjchem-1251	35	18	the	the	DET
eurjchem-1251	35	19	synthetic	synthetic	ADJ
eurjchem-1251	35	20	pathway	pathway	NOUN
eurjchem-1251	35	21	starting	start	VERB
eurjchem-1251	35	22	from	from	ADP
eurjchem-1251	35	23	benzilmono	benzilmono	PROPN
eurjchem-1251	35	24	hydrazine	hydrazine	NOUN
eurjchem-1251	35	25	and	and	CCONJ
eurjchem-1251	35	26	ethyl	ethyl	PROPN
eurjchem-1251	35	27	phenylacetate	phenylacetate	PROPN
eurjchem-1251	35	28	as	as	SCONJ
eurjchem-1251	35	29	described	describe	VERB
eurjchem-1251	35	30	in	in	ADP
eurjchem-1251	35	31	literature	literature	NOUN
eurjchem-1251	35	32	(	(	PUNCT
eurjchem-1251	35	33	scheme	scheme	NOUN
eurjchem-1251	35	34	1	1	NUM
eurjchem-1251	35	35	)	)	PUNCT
eurjchem-1251	36	1	[	[	X
eurjchem-1251	36	2	14	14	NUM
eurjchem-1251	36	3	]	]	SYM
eurjchem-1251	36	4	.	.	PUNCT
eurjchem-1251	37	1	2.2.2	2.2.2	X
eurjchem-1251	37	2	.	.	X
eurjchem-1251	38	1	synthesis	synthesis	NOUN
eurjchem-1251	38	2	of	of	ADP
eurjchem-1251	38	3	3‐chloro‐4,5,6‐triphenylpyridazine	3‐chloro‐4,5,6‐triphenylpyridazine	NUM
eurjchem-1251	38	4	(	(	PUNCT
eurjchem-1251	38	5	2	2	NUM
eurjchem-1251	38	6	)	)	PUNCT
eurjchem-1251	38	7	a	a	DET
eurjchem-1251	38	8	mixture	mixture	NOUN
eurjchem-1251	38	9	of	of	ADP
eurjchem-1251	38	10	compound	compound	NOUN
eurjchem-1251	38	11	1	1	NUM
eurjchem-1251	38	12	(	(	PUNCT
eurjchem-1251	38	13	0.5	0.5	NUM
eurjchem-1251	38	14	g	g	NOUN
eurjchem-1251	38	15	,	,	PUNCT
eurjchem-1251	38	16	1.54	1.54	NUM
eurjchem-1251	38	17	mmol	mmol	NOUN
eurjchem-1251	38	18	)	)	PUNCT
eurjchem-1251	38	19	and	and	CCONJ
eurjchem-1251	38	20	phosphoryl	phosphoryl	PROPN
eurjchem-1251	38	21	chloride	chloride	PROPN
eurjchem-1251	38	22	(	(	PUNCT
eurjchem-1251	38	23	10	10	NUM
eurjchem-1251	38	24	ml	ml	NOUN
eurjchem-1251	38	25	)	)	PUNCT
eurjchem-1251	38	26	was	be	AUX
eurjchem-1251	38	27	refluxed	refluxe	VERB
eurjchem-1251	38	28	for	for	ADP
eurjchem-1251	38	29	3	3	NUM
eurjchem-1251	38	30	hours	hour	NOUN
eurjchem-1251	38	31	,	,	PUNCT
eurjchem-1251	38	32	the	the	DET
eurjchem-1251	38	33	reaction	reaction	NOUN
eurjchem-1251	38	34	mixture	mixture	NOUN
eurjchem-1251	38	35	was	be	AUX
eurjchem-1251	38	36	cooled	cool	VERB
eurjchem-1251	38	37	and	and	CCONJ
eurjchem-1251	38	38	poured	pour	VERB
eurjchem-1251	38	39	into	into	ADP
eurjchem-1251	38	40	ice	ice	NOUN
eurjchem-1251	38	41	cooled	cool	VERB
eurjchem-1251	38	42	water	water	NOUN
eurjchem-1251	38	43	(	(	PUNCT
eurjchem-1251	38	44	100	100	NUM
eurjchem-1251	38	45	ml	ml	NOUN
eurjchem-1251	38	46	)	)	PUNCT
eurjchem-1251	38	47	.	.	PUNCT
eurjchem-1251	39	1	the	the	DET
eurjchem-1251	39	2	solid	solid	ADJ
eurjchem-1251	39	3	product	product	NOUN
eurjchem-1251	39	4	was	be	AUX
eurjchem-1251	39	5	filtered	filter	VERB
eurjchem-1251	39	6	off	off	ADP
eurjchem-1251	39	7	,	,	PUNCT
eurjchem-1251	39	8	washed	wash	VERB
eurjchem-1251	39	9	with	with	ADP
eurjchem-1251	39	10	water	water	NOUN
eurjchem-1251	39	11	,	,	PUNCT
eurjchem-1251	39	12	dried	dry	VERB
eurjchem-1251	39	13	and	and	CCONJ
eurjchem-1251	39	14	recrystallized	recrystallize	VERB
eurjchem-1251	39	15	from	from	ADP
eurjchem-1251	39	16	ethanol	ethanol	NOUN
eurjchem-1251	39	17	.	.	PUNCT
eurjchem-1251	40	1	m.p	m.p	PROPN
eurjchem-1251	40	2	.	.	PROPN
eurjchem-1251	40	3	:	:	PUNCT
eurjchem-1251	41	1	170‐172	170‐172	NUM
eurjchem-1251	41	2	°	°	ADP
eurjchem-1251	41	3	c	c	X
eurjchem-1251	41	4	(	(	PUNCT
eurjchem-1251	41	5	scheme	scheme	NOUN
eurjchem-1251	41	6	1	1	NUM
eurjchem-1251	41	7	)	)	PUNCT
eurjchem-1251	41	8	[	[	X
eurjchem-1251	41	9	14	14	NUM
eurjchem-1251	41	10	]	]	PUNCT
eurjchem-1251	41	11	.	.	PUNCT
eurjchem-1251	42	1	2.2.3	2.2.3	NUM
eurjchem-1251	42	2	.	.	X
eurjchem-1251	42	3	synthesis	synthesis	NOUN
eurjchem-1251	42	4	of	of	ADP
eurjchem-1251	42	5	6,7,8‐triphenyltetrazolo[1,5‐b]pyridazine	6,7,8‐triphenyltetrazolo[1,5‐b]pyridazine	NUM
eurjchem-1251	42	6	(	(	PUNCT
eurjchem-1251	42	7	3	3	NUM
eurjchem-1251	42	8	)	)	PUNCT
eurjchem-1251	42	9	to	to	ADP
eurjchem-1251	42	10	a	a	DET
eurjchem-1251	42	11	solution	solution	NOUN
eurjchem-1251	42	12	of	of	ADP
eurjchem-1251	42	13	compound	compound	NOUN
eurjchem-1251	42	14	2	2	NUM
eurjchem-1251	42	15	(	(	PUNCT
eurjchem-1251	42	16	0.5	0.5	NUM
eurjchem-1251	42	17	g	g	NOUN
eurjchem-1251	42	18	,	,	PUNCT
eurjchem-1251	42	19	1.46	1.46	NUM
eurjchem-1251	42	20	mmol	mmol	NOUN
eurjchem-1251	42	21	)	)	PUNCT
eurjchem-1251	42	22	in	in	ADP
eurjchem-1251	42	23	dimethylformamide	dimethylformamide	NOUN
eurjchem-1251	42	24	(	(	PUNCT
eurjchem-1251	42	25	10	10	NUM
eurjchem-1251	42	26	ml	ml	NOUN
eurjchem-1251	42	27	)	)	PUNCT
eurjchem-1251	42	28	sodium	sodium	NOUN
eurjchem-1251	42	29	azide	azide	NOUN
eurjchem-1251	42	30	(	(	PUNCT
eurjchem-1251	42	31	0.28	0.28	NUM
eurjchem-1251	42	32	g	g	NOUN
eurjchem-1251	42	33	,	,	PUNCT
eurjchem-1251	42	34	4.38	4.38	NUM
eurjchem-1251	42	35	mmol	mmol	NOUN
eurjchem-1251	42	36	)	)	PUNCT
eurjchem-1251	42	37	was	be	AUX
eurjchem-1251	42	38	added	add	VERB
eurjchem-1251	42	39	.	.	PUNCT
eurjchem-1251	43	1	the	the	DET
eurjchem-1251	43	2	reaction	reaction	NOUN
eurjchem-1251	43	3	mixture	mixture	NOUN
eurjchem-1251	43	4	was	be	AUX
eurjchem-1251	43	5	heated	heat	VERB
eurjchem-1251	43	6	at	at	ADP
eurjchem-1251	43	7	100	100	NUM
eurjchem-1251	43	8	°	°	ADP
eurjchem-1251	43	9	c	c	NOUN
eurjchem-1251	43	10	for	for	ADP
eurjchem-1251	43	11	1	1	NUM
eurjchem-1251	43	12	hour	hour	NOUN
eurjchem-1251	43	13	,	,	PUNCT
eurjchem-1251	43	14	the	the	DET
eurjchem-1251	43	15	cooled	cool	VERB
eurjchem-1251	43	16	reaction	reaction	NOUN
eurjchem-1251	43	17	mixture	mixture	NOUN
eurjchem-1251	43	18	was	be	AUX
eurjchem-1251	43	19	poured	pour	VERB
eurjchem-1251	43	20	into	into	ADP
eurjchem-1251	43	21	water	water	NOUN
eurjchem-1251	43	22	(	(	PUNCT
eurjchem-1251	43	23	100	100	NUM
eurjchem-1251	43	24	ml	ml	NOUN
eurjchem-1251	43	25	)	)	PUNCT
eurjchem-1251	43	26	,	,	PUNCT
eurjchem-1251	43	27	the	the	DET
eurjchem-1251	43	28	solid	solid	ADJ
eurjchem-1251	43	29	product	product	NOUN
eurjchem-1251	43	30	formed	form	VERB
eurjchem-1251	43	31	was	be	AUX
eurjchem-1251	43	32	filtered	filter	VERB
eurjchem-1251	43	33	off	off	ADP
eurjchem-1251	43	34	,	,	PUNCT
eurjchem-1251	43	35	washed	wash	VERB
eurjchem-1251	43	36	with	with	ADP
eurjchem-1251	43	37	water	water	NOUN
eurjchem-1251	43	38	,	,	PUNCT
eurjchem-1251	43	39	dried	dry	VERB
eurjchem-1251	43	40	and	and	CCONJ
eurjchem-1251	43	41	recrystallized	recrystallize	VERB
eurjchem-1251	43	42	from	from	ADP
eurjchem-1251	43	43	ethanol	ethanol	NOUN
eurjchem-1251	43	44	(	(	PUNCT
eurjchem-1251	43	45	scheme	scheme	NOUN
eurjchem-1251	43	46	1	1	NUM
eurjchem-1251	43	47	)	)	PUNCT
eurjchem-1251	43	48	.	.	PUNCT
eurjchem-1251	44	1	m.p	m.p	PROPN
eurjchem-1251	44	2	.	.	PROPN
eurjchem-1251	44	3	:	:	PUNCT
eurjchem-1251	45	1	194‐196	194‐196	NUM
eurjchem-1251	45	2	°	°	PRON
eurjchem-1251	45	3	c	c	X
eurjchem-1251	45	4	[	[	X
eurjchem-1251	45	5	15,16	15,16	NUM
eurjchem-1251	45	6	]	]	PUNCT
eurjchem-1251	45	7	.	.	PUNCT
eurjchem-1251	46	1	2.2.4	2.2.4	NUM
eurjchem-1251	46	2	.	.	X
eurjchem-1251	46	3	synthesis	synthesis	NOUN
eurjchem-1251	46	4	of	of	ADP
eurjchem-1251	46	5	4,5,6‐triphenyl‐n‐(triphenylphosphoran	4,5,6‐triphenyl‐n‐(triphenylphosphoran	NUM
eurjchem-1251	46	6	ylidene)pyridazine‐3‐amine	ylidene)pyridazine‐3‐amine	NOUN
eurjchem-1251	46	7	(	(	PUNCT
eurjchem-1251	46	8	4	4	NUM
eurjchem-1251	46	9	)	)	PUNCT
eurjchem-1251	46	10	to	to	ADP
eurjchem-1251	46	11	a	a	DET
eurjchem-1251	46	12	solution	solution	NOUN
eurjchem-1251	46	13	of	of	ADP
eurjchem-1251	46	14	compound	compound	NOUN
eurjchem-1251	46	15	3	3	NUM
eurjchem-1251	46	16	(	(	PUNCT
eurjchem-1251	46	17	0.5	0.5	NUM
eurjchem-1251	46	18	g	g	NOUN
eurjchem-1251	46	19	,	,	PUNCT
eurjchem-1251	46	20	1.43	1.43	NUM
eurjchem-1251	46	21	mmol	mmol	NOUN
eurjchem-1251	46	22	)	)	PUNCT
eurjchem-1251	46	23	in	in	ADP
eurjchem-1251	46	24	o‐	o‐	ADJ
eurjchem-1251	46	25	dichlorobenzene	dichlorobenzene	NOUN
eurjchem-1251	46	26	(	(	PUNCT
eurjchem-1251	46	27	10	10	NUM
eurjchem-1251	46	28	ml	ml	NOUN
eurjchem-1251	46	29	)	)	PUNCT
eurjchem-1251	46	30	,	,	PUNCT
eurjchem-1251	46	31	triphenylphosphine	triphenylphosphine	NOUN
eurjchem-1251	46	32	(	(	PUNCT
eurjchem-1251	46	33	0.37	0.37	NUM
eurjchem-1251	46	34	g	g	NOUN
eurjchem-1251	46	35	,	,	PUNCT
eurjchem-1251	46	36	1.43	1.43	NUM
eurjchem-1251	46	37	mmol	mmol	NOUN
eurjchem-1251	46	38	)	)	PUNCT
eurjchem-1251	46	39	was	be	AUX
eurjchem-1251	46	40	added	add	VERB
eurjchem-1251	46	41	.	.	PUNCT
eurjchem-1251	47	1	the	the	DET
eurjchem-1251	47	2	reaction	reaction	NOUN
eurjchem-1251	47	3	mixture	mixture	NOUN
eurjchem-1251	47	4	was	be	AUX
eurjchem-1251	47	5	refluxed	refluxe	VERB
eurjchem-1251	47	6	for	for	ADP
eurjchem-1251	47	7	3	3	NUM
eurjchem-1251	47	8	hours	hour	NOUN
eurjchem-1251	47	9	.	.	PUNCT
eurjchem-1251	48	1	the	the	DET
eurjchem-1251	48	2	solvent	solvent	NOUN
eurjchem-1251	48	3	was	be	AUX
eurjchem-1251	48	4	removed	remove	VERB
eurjchem-1251	48	5	under	under	ADP
eurjchem-1251	48	6	reduced	reduced	ADJ
eurjchem-1251	48	7	pressure	pressure	NOUN
eurjchem-1251	48	8	;	;	PUNCT
eurjchem-1251	48	9	the	the	DET
eurjchem-1251	48	10	residue	residue	NOUN
eurjchem-1251	48	11	was	be	AUX
eurjchem-1251	48	12	treated	treat	VERB
eurjchem-1251	48	13	with	with	ADP
eurjchem-1251	48	14	diethyl	diethyl	NOUN
eurjchem-1251	48	15	ether	ether	NOUN
eurjchem-1251	48	16	(	(	PUNCT
eurjchem-1251	48	17	30	30	NUM
eurjchem-1251	48	18	ml	ml	NOUN
eurjchem-1251	48	19	)	)	PUNCT
eurjchem-1251	48	20	.	.	PUNCT
eurjchem-1251	49	1	the	the	DET
eurjchem-1251	49	2	solid	solid	ADJ
eurjchem-1251	49	3	product	product	NOUN
eurjchem-1251	49	4	was	be	AUX
eurjchem-1251	49	5	filtered	filter	VERB
eurjchem-1251	49	6	off	off	ADP
eurjchem-1251	49	7	,	,	PUNCT
eurjchem-1251	49	8	dried	dry	VERB
eurjchem-1251	49	9	and	and	CCONJ
eurjchem-1251	49	10	recrystallized	recrystallize	VERB
eurjchem-1251	49	11	from	from	ADP
eurjchem-1251	49	12	acetone	acetone	NOUN
eurjchem-1251	49	13	similar	similar	ADJ
eurjchem-1251	49	14	to	to	ADP
eurjchem-1251	49	15	reported	report	VERB
eurjchem-1251	49	16	procedure	procedure	NOUN
eurjchem-1251	49	17	(	(	PUNCT
eurjchem-1251	49	18	scheme	scheme	NOUN
eurjchem-1251	49	19	1	1	NUM
eurjchem-1251	49	20	)	)	PUNCT
eurjchem-1251	50	1	[	[	X
eurjchem-1251	50	2	17	17	NUM
eurjchem-1251	50	3	]	]	PUNCT
eurjchem-1251	50	4	.	.	PUNCT
eurjchem-1251	51	1	color	color	NOUN
eurjchem-1251	51	2	:	:	PUNCT
eurjchem-1251	51	3	white	white	ADJ
eurjchem-1251	51	4	.	.	PUNCT
eurjchem-1251	52	1	yield	yield	NOUN
eurjchem-1251	52	2	:	:	PUNCT
eurjchem-1251	52	3	83	83	NUM
eurjchem-1251	52	4	%	%	NOUN
eurjchem-1251	52	5	.	.	PUNCT
eurjchem-1251	53	1	m.p	m.p	PROPN
eurjchem-1251	53	2	.	.	PROPN
eurjchem-1251	53	3	:	:	PUNCT
eurjchem-1251	54	1	248‐250	248‐250	NUM
eurjchem-1251	54	2	°	°	PROPN
eurjchem-1251	54	3	c	c	X
eurjchem-1251	54	4	.	.	PUNCT
eurjchem-1251	54	5	ft‐ir	ft‐ir	NOUN
eurjchem-1251	54	6	(	(	PUNCT
eurjchem-1251	54	7	kbr	kbr	PROPN
eurjchem-1251	54	8	,	,	PUNCT
eurjchem-1251	54	9	ν	ν	PROPN
eurjchem-1251	54	10	,	,	PUNCT
eurjchem-1251	54	11	cm‐1	cm‐1	PROPN
eurjchem-1251	54	12	):	):	PUNCT
eurjchem-1251	54	13	3055‐3023	3055‐3023	NUM
eurjchem-1251	54	14	(	(	PUNCT
eurjchem-1251	54	15	ch	ch	NOUN
eurjchem-1251	54	16	arom	arom	NOUN
eurjchem-1251	54	17	.	.	PUNCT
eurjchem-1251	54	18	)	)	PUNCT
eurjchem-1251	54	19	,	,	PUNCT
eurjchem-1251	54	20	1597	1597	NUM
eurjchem-1251	54	21	(	(	PUNCT
eurjchem-1251	54	22	c	c	NOUN
eurjchem-1251	54	23	=	=	SYM
eurjchem-1251	54	24	n	n	NUM
eurjchem-1251	54	25	)	)	PUNCT
eurjchem-1251	54	26	,	,	PUNCT
eurjchem-1251	54	27	1537	1537	NUM
eurjchem-1251	54	28	(	(	PUNCT
eurjchem-1251	54	29	p‐ph	p‐ph	PROPN
eurjchem-1251	54	30	)	)	PUNCT
eurjchem-1251	54	31	,	,	PUNCT
eurjchem-1251	54	32	1484	1484	NUM
eurjchem-1251	54	33	,	,	PUNCT
eurjchem-1251	54	34	1412	1412	NUM
eurjchem-1251	54	35	(	(	PUNCT
eurjchem-1251	54	36	c	c	NOUN
eurjchem-1251	54	37	=	=	SYM
eurjchem-1251	54	38	c	c	NOUN
eurjchem-1251	54	39	)	)	PUNCT
eurjchem-1251	54	40	.	.	PUNCT
eurjchem-1251	55	1	1h	1h	NUM
eurjchem-1251	55	2	nmr	nmr	NOUN
eurjchem-1251	55	3	(	(	PUNCT
eurjchem-1251	55	4	300	300	NUM
eurjchem-1251	55	5	mhz	mhz	NOUN
eurjchem-1251	55	6	,	,	PUNCT
eurjchem-1251	55	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	55	8	,	,	PUNCT
eurjchem-1251	55	9	δ	δ	PROPN
eurjchem-1251	55	10	,	,	PUNCT
eurjchem-1251	55	11	ppm	ppm	NOUN
eurjchem-1251	55	12	):	):	PUNCT
eurjchem-1251	55	13	7.93‐6.81	7.93‐6.81	NUM
eurjchem-1251	55	14	(	(	PUNCT
eurjchem-1251	55	15	m	m	PROPN
eurjchem-1251	55	16	,	,	PUNCT
eurjchem-1251	55	17	30h	30h	NOUN
eurjchem-1251	55	18	,	,	PUNCT
eurjchem-1251	55	19	6ph	6ph	ADJ
eurjchem-1251	55	20	)	)	PUNCT
eurjchem-1251	55	21	.	.	PUNCT
eurjchem-1251	56	1	ms	ms	NOUN
eurjchem-1251	56	2	(	(	PUNCT
eurjchem-1251	56	3	ei	ei	PROPN
eurjchem-1251	56	4	,	,	PUNCT
eurjchem-1251	56	5	m	m	PROPN
eurjchem-1251	56	6	/	/	SYM
eurjchem-1251	56	7	z	z	PROPN
eurjchem-1251	56	8	(	(	PUNCT
eurjchem-1251	56	9	%	%	NOUN
eurjchem-1251	56	10	)	)	PUNCT
eurjchem-1251	56	11	):	):	PUNCT
eurjchem-1251	56	12	583	583	NUM
eurjchem-1251	56	13	(	(	PUNCT
eurjchem-1251	56	14	m+	m+	NUM
eurjchem-1251	56	15	,	,	PUNCT
eurjchem-1251	56	16	100	100	NUM
eurjchem-1251	56	17	)	)	PUNCT
eurjchem-1251	56	18	.	.	PUNCT
eurjchem-1251	57	1	anal	anal	PROPN
eurjchem-1251	57	2	.	.	PUNCT
eurjchem-1251	57	3	calcd	calcd	NOUN
eurjchem-1251	57	4	.	.	PUNCT
eurjchem-1251	58	1	for	for	ADP
eurjchem-1251	58	2	c40h30n3p	c40h30n3p	VERB
eurjchem-1251	58	3	:	:	PUNCT
eurjchem-1251	58	4	c	c	X
eurjchem-1251	58	5	,	,	PUNCT
eurjchem-1251	58	6	82.31	82.31	NUM
eurjchem-1251	58	7	;	;	PUNCT
eurjchem-1251	58	8	h	h	NOUN
eurjchem-1251	58	9	,	,	PUNCT
eurjchem-1251	58	10	5.18	5.18	NUM
eurjchem-1251	58	11	;	;	PUNCT
eurjchem-1251	58	12	n	n	CCONJ
eurjchem-1251	58	13	,	,	PUNCT
eurjchem-1251	58	14	7.20	7.20	NUM
eurjchem-1251	58	15	.	.	PUNCT
eurjchem-1251	58	16	found	find	VERB
eurjchem-1251	58	17	:	:	PUNCT
eurjchem-1251	59	1	c	c	X
eurjchem-1251	59	2	,	,	PUNCT
eurjchem-1251	59	3	82.10	82.10	NUM
eurjchem-1251	59	4	;	;	PUNCT
eurjchem-1251	59	5	h	h	NOUN
eurjchem-1251	59	6	,	,	PUNCT
eurjchem-1251	59	7	5.00	5.00	NUM
eurjchem-1251	59	8	;	;	PUNCT
eurjchem-1251	59	9	n	n	CCONJ
eurjchem-1251	59	10	,	,	PUNCT
eurjchem-1251	59	11	7.00	7.00	NUM
eurjchem-1251	59	12	%	%	NOUN
eurjchem-1251	59	13	.	.	PUNCT
eurjchem-1251	60	1	2.2.5	2.2.5	X
eurjchem-1251	60	2	.	.	X
eurjchem-1251	60	3	synthesis	synthesis	NOUN
eurjchem-1251	60	4	of	of	ADP
eurjchem-1251	60	5	3‐amino‐4,5,6‐triphenylpyridazine	3‐amino‐4,5,6‐triphenylpyridazine	NUM
eurjchem-1251	60	6	(	(	PUNCT
eurjchem-1251	60	7	5	5	NUM
eurjchem-1251	60	8	)	)	PUNCT
eurjchem-1251	60	9	a	a	DET
eurjchem-1251	60	10	solution	solution	NOUN
eurjchem-1251	60	11	of	of	ADP
eurjchem-1251	60	12	compound	compound	NOUN
eurjchem-1251	60	13	4	4	NUM
eurjchem-1251	60	14	(	(	PUNCT
eurjchem-1251	60	15	0.5	0.5	NUM
eurjchem-1251	60	16	g	g	NOUN
eurjchem-1251	60	17	,	,	PUNCT
eurjchem-1251	60	18	0.86	0.86	NUM
eurjchem-1251	60	19	mmol	mmol	NOUN
eurjchem-1251	60	20	)	)	PUNCT
eurjchem-1251	60	21	in	in	ADP
eurjchem-1251	60	22	acoh	acoh	ADJ
eurjchem-1251	60	23	(	(	PUNCT
eurjchem-1251	60	24	80	80	NUM
eurjchem-1251	60	25	%	%	NOUN
eurjchem-1251	60	26	,	,	PUNCT
eurjchem-1251	60	27	10	10	NUM
eurjchem-1251	60	28	ml	ml	NOUN
eurjchem-1251	60	29	)	)	PUNCT
eurjchem-1251	60	30	was	be	AUX
eurjchem-1251	60	31	heated	heat	VERB
eurjchem-1251	60	32	under	under	ADP
eurjchem-1251	60	33	reflux	reflux	NOUN
eurjchem-1251	60	34	for	for	ADP
eurjchem-1251	60	35	1	1	NUM
eurjchem-1251	60	36	h.	h.	NOUN
eurjchem-1251	60	37	after	after	ADP
eurjchem-1251	60	38	cooling	cool	VERB
eurjchem-1251	60	39	,	,	PUNCT
eurjchem-1251	60	40	the	the	DET
eurjchem-1251	60	41	reaction	reaction	NOUN
eurjchem-1251	60	42	mixture	mixture	NOUN
eurjchem-1251	60	43	was	be	AUX
eurjchem-1251	60	44	poured	pour	VERB
eurjchem-1251	60	45	into	into	ADP
eurjchem-1251	60	46	water	water	NOUN
eurjchem-1251	60	47	(	(	PUNCT
eurjchem-1251	60	48	100	100	NUM
eurjchem-1251	60	49	ml	ml	NOUN
eurjchem-1251	60	50	)	)	PUNCT
eurjchem-1251	60	51	.	.	PUNCT
eurjchem-1251	61	1	the	the	DET
eurjchem-1251	61	2	precipitate	precipitate	NOUN
eurjchem-1251	61	3	that	that	PRON
eurjchem-1251	61	4	formed	form	VERB
eurjchem-1251	61	5	was	be	AUX
eurjchem-1251	61	6	filtered	filter	VERB
eurjchem-1251	61	7	off	off	ADP
eurjchem-1251	61	8	,	,	PUNCT
eurjchem-1251	61	9	washed	wash	VERB
eurjchem-1251	61	10	with	with	ADP
eurjchem-1251	61	11	water	water	NOUN
eurjchem-1251	61	12	,	,	PUNCT
eurjchem-1251	61	13	dried	dry	VERB
eurjchem-1251	61	14	,	,	PUNCT
eurjchem-1251	61	15	and	and	CCONJ
eurjchem-1251	61	16	recrystallized	recrystallize	VERB
eurjchem-1251	61	17	from	from	ADP
eurjchem-1251	61	18	methanol	methanol	NOUN
eurjchem-1251	61	19	(	(	PUNCT
eurjchem-1251	61	20	scheme	scheme	NOUN
eurjchem-1251	61	21	1	1	NUM
eurjchem-1251	61	22	)	)	PUNCT
eurjchem-1251	61	23	.	.	PUNCT
eurjchem-1251	62	1	color	color	NOUN
eurjchem-1251	62	2	:	:	PUNCT
eurjchem-1251	62	3	white	white	ADJ
eurjchem-1251	62	4	.	.	PUNCT
eurjchem-1251	63	1	yield	yield	NOUN
eurjchem-1251	63	2	:	:	PUNCT
eurjchem-1251	63	3	86.61	86.61	NUM
eurjchem-1251	63	4	%	%	NOUN
eurjchem-1251	63	5	.	.	PUNCT
eurjchem-1251	64	1	m.p	m.p	PROPN
eurjchem-1251	64	2	.	.	PROPN
eurjchem-1251	64	3	:	:	PUNCT
eurjchem-1251	65	1	260‐262	260‐262	NUM
eurjchem-1251	65	2	°	°	ADP
eurjchem-1251	65	3	c	c	X
eurjchem-1251	65	4	.	.	PUNCT
eurjchem-1251	65	5	ft‐ir	ft‐ir	NOUN
eurjchem-1251	65	6	(	(	PUNCT
eurjchem-1251	65	7	kbr	kbr	PROPN
eurjchem-1251	65	8	,	,	PUNCT
eurjchem-1251	65	9	ν	ν	PROPN
eurjchem-1251	65	10	,	,	PUNCT
eurjchem-1251	65	11	cm‐1	cm‐1	PROPN
eurjchem-1251	65	12	):	):	PUNCT
eurjchem-1251	65	13	3470‐3280	3470‐3280	NUM
eurjchem-1251	65	14	(	(	PUNCT
eurjchem-1251	65	15	nh2	nh2	PROPN
eurjchem-1251	65	16	)	)	PUNCT
eurjchem-1251	65	17	,	,	PUNCT
eurjchem-1251	65	18	3059	3059	NUM
eurjchem-1251	65	19	(	(	PUNCT
eurjchem-1251	65	20	ch	ch	NOUN
eurjchem-1251	65	21	arom	arom	NOUN
eurjchem-1251	65	22	.	.	PUNCT
eurjchem-1251	65	23	)	)	PUNCT
eurjchem-1251	65	24	,	,	PUNCT
eurjchem-1251	65	25	1629	1629	NUM
eurjchem-1251	65	26	(	(	PUNCT
eurjchem-1251	65	27	c	c	NOUN
eurjchem-1251	65	28	=	=	SYM
eurjchem-1251	65	29	n	n	NUM
eurjchem-1251	65	30	)	)	PUNCT
eurjchem-1251	65	31	.	.	PUNCT
eurjchem-1251	66	1	1h	1h	NUM
eurjchem-1251	66	2	nmr	nmr	NOUN
eurjchem-1251	66	3	(	(	PUNCT
eurjchem-1251	66	4	300	300	NUM
eurjchem-1251	66	5	mhz	mhz	NOUN
eurjchem-1251	66	6	,	,	PUNCT
eurjchem-1251	66	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	66	8	,	,	PUNCT
eurjchem-1251	66	9	δ	δ	PROPN
eurjchem-1251	66	10	,	,	PUNCT
eurjchem-1251	66	11	ppm	ppm	NUM
eurjchem-1251	66	12	):	):	PUNCT
eurjchem-1251	66	13	5.84	5.84	NUM
eurjchem-1251	66	14	(	(	PUNCT
eurjchem-1251	66	15	s	s	PROPN
eurjchem-1251	66	16	,	,	PUNCT
eurjchem-1251	66	17	2h	2h	NUM
eurjchem-1251	66	18	,	,	PUNCT
eurjchem-1251	66	19	nh2	nh2	PROPN
eurjchem-1251	66	20	)	)	PUNCT
eurjchem-1251	66	21	,	,	PUNCT
eurjchem-1251	66	22	6.87‐7.62	6.87‐7.62	NUM
eurjchem-1251	66	23	(	(	PUNCT
eurjchem-1251	66	24	m	m	PROPN
eurjchem-1251	66	25	,	,	PUNCT
eurjchem-1251	66	26	15h	15h	NUM
eurjchem-1251	66	27	,	,	PUNCT
eurjchem-1251	66	28	3ph	3ph	NOUN
eurjchem-1251	66	29	)	)	PUNCT
eurjchem-1251	66	30	.	.	PUNCT
eurjchem-1251	67	1	ms	ms	NOUN
eurjchem-1251	67	2	(	(	PUNCT
eurjchem-1251	67	3	ei	ei	PROPN
eurjchem-1251	67	4	,	,	PUNCT
eurjchem-1251	67	5	m	m	PROPN
eurjchem-1251	67	6	/	/	SYM
eurjchem-1251	67	7	z	z	PROPN
eurjchem-1251	67	8	(	(	PUNCT
eurjchem-1251	67	9	%	%	NOUN
eurjchem-1251	67	10	)	)	PUNCT
eurjchem-1251	67	11	):	):	PUNCT
eurjchem-1251	67	12	323([m]+	323([m]+	NUM
eurjchem-1251	67	13	,	,	PUNCT
eurjchem-1251	67	14	58.23	58.23	NUM
eurjchem-1251	67	15	)	)	PUNCT
eurjchem-1251	67	16	,	,	PUNCT
eurjchem-1251	67	17	322	322	NUM
eurjchem-1251	67	18	(	(	PUNCT
eurjchem-1251	67	19	[	[	X
eurjchem-1251	67	20	m‐1]+	m‐1]+	X
eurjchem-1251	67	21	(	(	PUNCT
eurjchem-1251	67	22	100	100	NUM
eurjchem-1251	67	23	)	)	PUNCT
eurjchem-1251	67	24	)	)	PUNCT
eurjchem-1251	67	25	,	,	PUNCT
eurjchem-1251	67	26	246	246	NUM
eurjchem-1251	67	27	(	(	PUNCT
eurjchem-1251	67	28	3.82	3.82	NUM
eurjchem-1251	67	29	)	)	PUNCT
eurjchem-1251	67	30	,	,	PUNCT
eurjchem-1251	67	31	178	178	NUM
eurjchem-1251	67	32	(	(	PUNCT
eurjchem-1251	67	33	15.05	15.05	NUM
eurjchem-1251	67	34	)	)	PUNCT
eurjchem-1251	67	35	,	,	PUNCT
eurjchem-1251	67	36	146	146	NUM
eurjchem-1251	67	37	(	(	PUNCT
eurjchem-1251	67	38	2.10	2.10	NUM
eurjchem-1251	67	39	)	)	PUNCT
eurjchem-1251	67	40	,	,	PUNCT
eurjchem-1251	67	41	117	117	NUM
eurjchem-1251	67	42	(	(	PUNCT
eurjchem-1251	67	43	36.06	36.06	NUM
eurjchem-1251	67	44	)	)	PUNCT
eurjchem-1251	67	45	,	,	PUNCT
eurjchem-1251	67	46	103	103	NUM
eurjchem-1251	67	47	(	(	PUNCT
eurjchem-1251	67	48	1.31	1.31	NUM
eurjchem-1251	67	49	)	)	PUNCT
eurjchem-1251	67	50	,	,	PUNCT
eurjchem-1251	67	51	77	77	NUM
eurjchem-1251	67	52	(	(	PUNCT
eurjchem-1251	67	53	5.93	5.93	NUM
eurjchem-1251	67	54	)	)	PUNCT
eurjchem-1251	67	55	.	.	PUNCT
eurjchem-1251	68	1	anal.calcd	anal.calcd	PROPN
eurjchem-1251	68	2	.	.	PROPN
eurjchem-1251	69	1	for	for	ADP
eurjchem-1251	69	2	c22h17n3	c22h17n3	PROPN
eurjchem-1251	69	3	:	:	PUNCT
eurjchem-1251	69	4	c	c	X
eurjchem-1251	69	5	,	,	PUNCT
eurjchem-1251	69	6	81.71	81.71	NUM
eurjchem-1251	69	7	;	;	PUNCT
eurjchem-1251	70	1	h	h	NOUN
eurjchem-1251	70	2	,	,	PUNCT
eurjchem-1251	70	3	5.30	5.30	NUM
eurjchem-1251	70	4	;	;	PUNCT
eurjchem-1251	70	5	n	n	CCONJ
eurjchem-1251	70	6	,	,	PUNCT
eurjchem-1251	70	7	12.99	12.99	NUM
eurjchem-1251	70	8	.	.	PUNCT
eurjchem-1251	70	9	found	find	VERB
eurjchem-1251	70	10	:	:	PUNCT
eurjchem-1251	71	1	c	c	X
eurjchem-1251	71	2	,	,	PUNCT
eurjchem-1251	71	3	81.70	81.70	NUM
eurjchem-1251	71	4	;	;	PUNCT
eurjchem-1251	71	5	h	h	PROPN
eurjchem-1251	71	6	5.30	5.30	NUM
eurjchem-1251	71	7	;	;	PUNCT
eurjchem-1251	71	8	n	n	DET
eurjchem-1251	71	9	12.90	12.90	NUM
eurjchem-1251	71	10	%	%	NOUN
eurjchem-1251	71	11	.	.	PUNCT
eurjchem-1251	72	1	2.2.5.1	2.2.5.1	X
eurjchem-1251	72	2	.	.	PUNCT
eurjchem-1251	73	1	reaction	reaction	NOUN
eurjchem-1251	73	2	of	of	ADP
eurjchem-1251	73	3	compound	compound	NOUN
eurjchem-1251	73	4	5	5	NUM
eurjchem-1251	73	5	with	with	ADP
eurjchem-1251	73	6	nitrous	nitrous	ADJ
eurjchem-1251	73	7	acid	acid	NOUN
eurjchem-1251	73	8	compound	compound	NOUN
eurjchem-1251	73	9	5	5	NUM
eurjchem-1251	73	10	(	(	PUNCT
eurjchem-1251	73	11	0.5	0.5	NUM
eurjchem-1251	73	12	g,1.55	g,1.55	PROPN
eurjchem-1251	73	13	mmol	mmol	NOUN
eurjchem-1251	73	14	)	)	PUNCT
eurjchem-1251	73	15	was	be	AUX
eurjchem-1251	73	16	dissolved	dissolve	VERB
eurjchem-1251	73	17	in	in	ADP
eurjchem-1251	73	18	concentrated	concentrated	ADJ
eurjchem-1251	73	19	hcl	hcl	PROPN
eurjchem-1251	73	20	(	(	PUNCT
eurjchem-1251	73	21	5	5	NUM
eurjchem-1251	73	22	ml	ml	NOUN
eurjchem-1251	73	23	)	)	PUNCT
eurjchem-1251	73	24	,	,	PUNCT
eurjchem-1251	73	25	cooled	cool	VERB
eurjchem-1251	73	26	to	to	ADP
eurjchem-1251	73	27	0‐5	0‐5	NUM
eurjchem-1251	73	28	°	°	ADP
eurjchem-1251	73	29	c	c	NOUN
eurjchem-1251	73	30	in	in	ADP
eurjchem-1251	73	31	an	an	DET
eurjchem-1251	73	32	ice	ice	NOUN
eurjchem-1251	73	33	bath	bath	NOUN
eurjchem-1251	73	34	,	,	PUNCT
eurjchem-1251	73	35	then	then	ADV
eurjchem-1251	73	36	a	a	DET
eurjchem-1251	73	37	solution	solution	NOUN
eurjchem-1251	73	38	of	of	ADP
eurjchem-1251	73	39	nano2	nano2	NOUN
eurjchem-1251	73	40	(	(	PUNCT
eurjchem-1251	73	41	0.22	0.22	NUM
eurjchem-1251	73	42	g	g	NOUN
eurjchem-1251	73	43	,	,	PUNCT
eurjchem-1251	73	44	3.1	3.1	NUM
eurjchem-1251	73	45	mmol	mmol	NOUN
eurjchem-1251	73	46	)	)	PUNCT
eurjchem-1251	73	47	in	in	ADP
eurjchem-1251	73	48	h2o	h2o	PROPN
eurjchem-1251	73	49	(	(	PUNCT
eurjchem-1251	73	50	5	5	NUM
eurjchem-1251	73	51	ml	ml	NOUN
eurjchem-1251	73	52	)	)	PUNCT
eurjchem-1251	73	53	was	be	AUX
eurjchem-1251	73	54	added	add	VERB
eurjchem-1251	73	55	drop	drop	NOUN
eurjchem-1251	73	56	by	by	ADP
eurjchem-1251	73	57	drop	drop	NOUN
eurjchem-1251	73	58	with	with	ADP
eurjchem-1251	73	59	stirring	stirring	NOUN
eurjchem-1251	73	60	,	,	PUNCT
eurjchem-1251	73	61	keeping	keep	VERB
eurjchem-1251	73	62	the	the	DET
eurjchem-1251	73	63	temperature	temperature	NOUN
eurjchem-1251	73	64	at	at	ADP
eurjchem-1251	73	65	0‐5	0‐5	NOUN
eurjchem-1251	73	66	°	°	ADP
eurjchem-1251	73	67	c	c	X
eurjchem-1251	73	68	.	.	PUNCT
eurjchem-1251	74	1	the	the	DET
eurjchem-1251	74	2	mixture	mixture	NOUN
eurjchem-1251	74	3	was	be	AUX
eurjchem-1251	74	4	stirred	stir	VERB
eurjchem-1251	74	5	for	for	ADP
eurjchem-1251	74	6	further	further	ADJ
eurjchem-1251	74	7	1	1	NUM
eurjchem-1251	74	8	h	h	NOUN
eurjchem-1251	74	9	at	at	ADP
eurjchem-1251	74	10	room	room	NOUN
eurjchem-1251	74	11	temperature	temperature	NOUN
eurjchem-1251	74	12	.	.	PUNCT
eurjchem-1251	75	1	the	the	DET
eurjchem-1251	75	2	solid	solid	ADJ
eurjchem-1251	75	3	product	product	NOUN
eurjchem-1251	75	4	was	be	AUX
eurjchem-1251	75	5	filtered	filter	VERB
eurjchem-1251	75	6	off	off	ADP
eurjchem-1251	75	7	,	,	PUNCT
eurjchem-1251	75	8	washed	wash	VERB
eurjchem-1251	75	9	with	with	ADP
eurjchem-1251	75	10	water	water	NOUN
eurjchem-1251	75	11	,	,	PUNCT
eurjchem-1251	75	12	dried	dry	VERB
eurjchem-1251	75	13	and	and	CCONJ
eurjchem-1251	75	14	recrystallized	recrystallize	VERB
eurjchem-1251	75	15	from	from	ADP
eurjchem-1251	75	16	benzene	benzene	NOUN
eurjchem-1251	75	17	to	to	PART
eurjchem-1251	75	18	give	give	VERB
eurjchem-1251	75	19	compound	compound	NOUN
eurjchem-1251	75	20	1	1	NUM
eurjchem-1251	75	21	,	,	PUNCT
eurjchem-1251	75	22	identical	identical	ADJ
eurjchem-1251	75	23	with	with	ADP
eurjchem-1251	75	24	that	that	PRON
eurjchem-1251	75	25	prepared	prepare	VERB
eurjchem-1251	75	26	from	from	ADP
eurjchem-1251	75	27	benzilmonohydrazone	benzilmonohydrazone	NOUN
eurjchem-1251	75	28	and	and	CCONJ
eurjchem-1251	75	29	ethyl	ethyl	PROPN
eurjchem-1251	75	30	phenyl	phenyl	NOUN
eurjchem-1251	75	31	acetate	acetate	NOUN
eurjchem-1251	75	32	,	,	PUNCT
eurjchem-1251	75	33	according	accord	VERB
eurjchem-1251	75	34	to	to	ADP
eurjchem-1251	75	35	reference	reference	NOUN
eurjchem-1251	75	36	(	(	PUNCT
eurjchem-1251	75	37	scheme	scheme	NOUN
eurjchem-1251	75	38	1	1	NUM
eurjchem-1251	75	39	)	)	PUNCT
eurjchem-1251	76	1	[	[	X
eurjchem-1251	76	2	14	14	NUM
eurjchem-1251	76	3	]	]	X
eurjchem-1251	76	4	(	(	PUNCT
eurjchem-1251	76	5	m.p	m.p	AUX
eurjchem-1251	76	6	.	.	PROPN
eurjchem-1251	76	7	and	and	CCONJ
eurjchem-1251	76	8	mixed	mixed	ADJ
eurjchem-1251	76	9	m.p	m.p	PROPN
eurjchem-1251	76	10	.	.	PROPN
eurjchem-1251	76	11	)	)	PUNCT
eurjchem-1251	76	12	.	.	PUNCT
eurjchem-1251	77	1	yield	yield	NOUN
eurjchem-1251	77	2	:	:	PUNCT
eurjchem-1251	77	3	0.43	0.43	NUM
eurjchem-1251	77	4	g	g	NOUN
eurjchem-1251	77	5	(	(	PUNCT
eurjchem-1251	77	6	85.66	85.66	NUM
eurjchem-1251	77	7	%	%	NOUN
eurjchem-1251	77	8	)	)	PUNCT
eurjchem-1251	77	9	.	.	PUNCT
eurjchem-1251	78	1	2.2.6	2.2.6	X
eurjchem-1251	78	2	.	.	PUNCT
eurjchem-1251	78	3	synthesis	synthesis	NOUN
eurjchem-1251	78	4	of	of	ADP
eurjchem-1251	78	5	n‐(4,5,6‐triphenylpyridazin‐3‐yl	n‐(4,5,6‐triphenylpyridazin‐3‐yl	PROPN
eurjchem-1251	78	6	)	)	PUNCT
eurjchem-1251	78	7	formamide	formamide	ADV
eurjchem-1251	78	8	(	(	PUNCT
eurjchem-1251	78	9	6a	6a	NOUN
eurjchem-1251	78	10	)	)	PUNCT
eurjchem-1251	78	11	a	a	DET
eurjchem-1251	78	12	mixture	mixture	NOUN
eurjchem-1251	78	13	of	of	ADP
eurjchem-1251	78	14	compound	compound	NOUN
eurjchem-1251	78	15	5	5	NUM
eurjchem-1251	78	16	(	(	PUNCT
eurjchem-1251	78	17	0.5	0.5	NUM
eurjchem-1251	78	18	g	g	NOUN
eurjchem-1251	78	19	,	,	PUNCT
eurjchem-1251	78	20	1.55	1.55	NUM
eurjchem-1251	78	21	mmol	mmol	NOUN
eurjchem-1251	78	22	)	)	PUNCT
eurjchem-1251	78	23	and	and	CCONJ
eurjchem-1251	78	24	formic	formic	PROPN
eurjchem-1251	78	25	acid	acid	NOUN
eurjchem-1251	78	26	(	(	PUNCT
eurjchem-1251	78	27	0.1	0.1	NUM
eurjchem-1251	78	28	ml	ml	NOUN
eurjchem-1251	78	29	,	,	PUNCT
eurjchem-1251	78	30	1.55	1.55	NUM
eurjchem-1251	78	31	mmol	mmol	NOUN
eurjchem-1251	78	32	)	)	PUNCT
eurjchem-1251	78	33	in	in	ADP
eurjchem-1251	78	34	dimethylformamide	dimethylformamide	NOUN
eurjchem-1251	78	35	(	(	PUNCT
eurjchem-1251	78	36	10	10	NUM
eurjchem-1251	78	37	ml	ml	NOUN
eurjchem-1251	78	38	)	)	PUNCT
eurjchem-1251	78	39	was	be	AUX
eurjchem-1251	78	40	refluxed	refluxe	VERB
eurjchem-1251	78	41	for	for	ADP
eurjchem-1251	78	42	7	7	NUM
eurjchem-1251	78	43	h.	h.	NOUN
eurjchem-1251	78	44	after	after	ADP
eurjchem-1251	78	45	cooling	cool	VERB
eurjchem-1251	78	46	,	,	PUNCT
eurjchem-1251	78	47	the	the	DET
eurjchem-1251	78	48	reaction	reaction	NOUN
eurjchem-1251	78	49	mixture	mixture	NOUN
eurjchem-1251	78	50	was	be	AUX
eurjchem-1251	78	51	poured	pour	VERB
eurjchem-1251	78	52	into	into	ADP
eurjchem-1251	78	53	ice	ice	NOUN
eurjchem-1251	78	54	water	water	NOUN
eurjchem-1251	78	55	(	(	PUNCT
eurjchem-1251	78	56	100	100	NUM
eurjchem-1251	78	57	ml	ml	NOUN
eurjchem-1251	78	58	)	)	PUNCT
eurjchem-1251	78	59	.	.	PUNCT
eurjchem-1251	79	1	the	the	DET
eurjchem-1251	79	2	precipitate	precipitate	NOUN
eurjchem-1251	79	3	that	that	PRON
eurjchem-1251	79	4	formed	form	VERB
eurjchem-1251	79	5	was	be	AUX
eurjchem-1251	79	6	filtered	filter	VERB
eurjchem-1251	79	7	off	off	ADP
eurjchem-1251	79	8	,	,	PUNCT
eurjchem-1251	79	9	washed	wash	VERB
eurjchem-1251	79	10	with	with	ADP
eurjchem-1251	79	11	water	water	NOUN
eurjchem-1251	79	12	,	,	PUNCT
eurjchem-1251	79	13	dried	dry	VERB
eurjchem-1251	79	14	,	,	PUNCT
eurjchem-1251	79	15	and	and	CCONJ
eurjchem-1251	79	16	recrystallized	recrystallize	VERB
eurjchem-1251	79	17	from	from	ADP
eurjchem-1251	79	18	ethanol	ethanol	NOUN
eurjchem-1251	79	19	(	(	PUNCT
eurjchem-1251	79	20	scheme	scheme	NOUN
eurjchem-1251	79	21	2	2	NUM
eurjchem-1251	79	22	)	)	PUNCT
eurjchem-1251	79	23	.	.	PUNCT
eurjchem-1251	80	1	color	color	NOUN
eurjchem-1251	80	2	:	:	PUNCT
eurjchem-1251	80	3	white	white	ADJ
eurjchem-1251	80	4	.	.	PUNCT
eurjchem-1251	81	1	yield	yield	NOUN
eurjchem-1251	81	2	:	:	PUNCT
eurjchem-1251	81	3	92	92	NUM
eurjchem-1251	81	4	%	%	NOUN
eurjchem-1251	81	5	.	.	PUNCT
eurjchem-1251	82	1	m.p	m.p	PROPN
eurjchem-1251	82	2	.	.	PROPN
eurjchem-1251	82	3	:	:	PUNCT
eurjchem-1251	83	1	237‐	237‐	NUM
eurjchem-1251	83	2	238	238	NUM
eurjchem-1251	83	3	°	°	NOUN
eurjchem-1251	83	4	c	c	X
eurjchem-1251	83	5	.	.	PUNCT
eurjchem-1251	84	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	84	2	(	(	PUNCT
eurjchem-1251	84	3	kbr	kbr	PROPN
eurjchem-1251	84	4	,	,	PUNCT
eurjchem-1251	84	5	ν	ν	PROPN
eurjchem-1251	84	6	,	,	PUNCT
eurjchem-1251	84	7	cm‐1	cm‐1	PROPN
eurjchem-1251	84	8	):	):	PUNCT
eurjchem-1251	84	9	3279	3279	NUM
eurjchem-1251	84	10	(	(	PUNCT
eurjchem-1251	84	11	nh	nh	NOUN
eurjchem-1251	84	12	)	)	PUNCT
eurjchem-1251	84	13	,	,	PUNCT
eurjchem-1251	84	14	3058	3058	NUM
eurjchem-1251	84	15	(	(	PUNCT
eurjchem-1251	84	16	ch	ch	NOUN
eurjchem-1251	84	17	arom	arom	NOUN
eurjchem-1251	84	18	.	.	PUNCT
eurjchem-1251	84	19	)	)	PUNCT
eurjchem-1251	84	20	,	,	PUNCT
eurjchem-1251	84	21	1697	1697	NUM
eurjchem-1251	84	22	(	(	PUNCT
eurjchem-1251	84	23	c	c	NOUN
eurjchem-1251	84	24	=	=	NOUN
eurjchem-1251	84	25	o	o	NOUN
eurjchem-1251	84	26	)	)	PUNCT
eurjchem-1251	84	27	,	,	PUNCT
eurjchem-1251	84	28	1629	1629	NUM
eurjchem-1251	84	29	(	(	PUNCT
eurjchem-1251	84	30	c	c	NOUN
eurjchem-1251	84	31	=	=	SYM
eurjchem-1251	84	32	n	n	NUM
eurjchem-1251	84	33	)	)	PUNCT
eurjchem-1251	84	34	.	.	PUNCT
eurjchem-1251	85	1	1h	1h	NUM
eurjchem-1251	85	2	nmr	nmr	NOUN
eurjchem-1251	85	3	(	(	PUNCT
eurjchem-1251	85	4	300	300	NUM
eurjchem-1251	85	5	mhz	mhz	NOUN
eurjchem-1251	85	6	,	,	PUNCT
eurjchem-1251	85	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	85	8	,	,	PUNCT
eurjchem-1251	85	9	δ	δ	PROPN
eurjchem-1251	85	10	,	,	PUNCT
eurjchem-1251	85	11	ppm	ppm	NUM
eurjchem-1251	85	12	):	):	PUNCT
eurjchem-1251	85	13	5.78	5.78	NUM
eurjchem-1251	85	14	(	(	PUNCT
eurjchem-1251	85	15	s	s	PROPN
eurjchem-1251	85	16	,	,	PUNCT
eurjchem-1251	85	17	1h	1h	NUM
eurjchem-1251	85	18	,	,	PUNCT
eurjchem-1251	85	19	nh	nh	PROPN
eurjchem-1251	85	20	)	)	PUNCT
eurjchem-1251	85	21	,	,	PUNCT
eurjchem-1251	85	22	6.99‐7.09	6.99‐7.09	NUM
eurjchem-1251	85	23	(	(	PUNCT
eurjchem-1251	85	24	m	m	PROPN
eurjchem-1251	85	25	,	,	PUNCT
eurjchem-1251	85	26	15h	15h	NUM
eurjchem-1251	85	27	,	,	PUNCT
eurjchem-1251	85	28	3ph	3ph	NOUN
eurjchem-1251	85	29	)	)	PUNCT
eurjchem-1251	85	30	,	,	PUNCT
eurjchem-1251	85	31	7.14	7.14	NUM
eurjchem-1251	85	32	(	(	PUNCT
eurjchem-1251	85	33	s	s	PROPN
eurjchem-1251	85	34	,	,	PUNCT
eurjchem-1251	85	35	1h	1h	NUM
eurjchem-1251	85	36	,	,	PUNCT
eurjchem-1251	85	37	cho	cho	NOUN
eurjchem-1251	85	38	)	)	PUNCT
eurjchem-1251	85	39	.	.	PUNCT
eurjchem-1251	86	1	ms	ms	NOUN
eurjchem-1251	86	2	(	(	PUNCT
eurjchem-1251	86	3	ei	ei	PROPN
eurjchem-1251	86	4	,	,	PUNCT
eurjchem-1251	86	5	m	m	PROPN
eurjchem-1251	86	6	/	/	SYM
eurjchem-1251	86	7	z	z	PROPN
eurjchem-1251	86	8	(	(	PUNCT
eurjchem-1251	86	9	%	%	NOUN
eurjchem-1251	86	10	)	)	PUNCT
eurjchem-1251	86	11	):	):	PUNCT
eurjchem-1251	86	12	351	351	NUM
eurjchem-1251	86	13	(	(	PUNCT
eurjchem-1251	86	14	[	[	X
eurjchem-1251	86	15	m]+	m]+	NOUN
eurjchem-1251	86	16	,	,	PUNCT
eurjchem-1251	86	17	2.37	2.37	NUM
eurjchem-1251	86	18	)	)	PUNCT
eurjchem-1251	86	19	,	,	PUNCT
eurjchem-1251	86	20	322	322	NUM
eurjchem-1251	86	21	(	(	PUNCT
eurjchem-1251	86	22	[	[	X
eurjchem-1251	86	23	m‐29]+	m‐29]+	NOUN
eurjchem-1251	86	24	,	,	PUNCT
eurjchem-1251	86	25	100	100	NUM
eurjchem-1251	86	26	)	)	PUNCT
eurjchem-1251	86	27	,	,	PUNCT
eurjchem-1251	86	28	246	246	NUM
eurjchem-1251	86	29	(	(	PUNCT
eurjchem-1251	86	30	3.82	3.82	NUM
eurjchem-1251	86	31	)	)	PUNCT
eurjchem-1251	86	32	,	,	PUNCT
eurjchem-1251	86	33	178	178	NUM
eurjchem-1251	86	34	(	(	PUNCT
eurjchem-1251	86	35	15.05	15.05	NUM
eurjchem-1251	86	36	)	)	PUNCT
eurjchem-1251	86	37	,	,	PUNCT
eurjchem-1251	86	38	146	146	NUM
eurjchem-1251	86	39	(	(	PUNCT
eurjchem-1251	86	40	2.10	2.10	NUM
eurjchem-1251	86	41	)	)	PUNCT
eurjchem-1251	86	42	,	,	PUNCT
eurjchem-1251	86	43	117	117	NUM
eurjchem-1251	86	44	(	(	PUNCT
eurjchem-1251	86	45	36.06	36.06	NUM
eurjchem-1251	86	46	)	)	PUNCT
eurjchem-1251	86	47	,	,	PUNCT
eurjchem-1251	86	48	103	103	NUM
eurjchem-1251	86	49	(	(	PUNCT
eurjchem-1251	86	50	1.31	1.31	NUM
eurjchem-1251	86	51	)	)	PUNCT
eurjchem-1251	86	52	.	.	PUNCT
eurjchem-1251	87	1	anal	anal	PROPN
eurjchem-1251	87	2	.	.	PUNCT
eurjchem-1251	87	3	calcd	calcd	NOUN
eurjchem-1251	87	4	.	.	PUNCT
eurjchem-1251	88	1	for	for	ADP
eurjchem-1251	88	2	c23h17n3o	c23h17n3o	NOUN
eurjchem-1251	88	3	:	:	PUNCT
eurjchem-1251	88	4	c	c	X
eurjchem-1251	88	5	,	,	PUNCT
eurjchem-1251	88	6	78.61	78.61	NUM
eurjchem-1251	88	7	;	;	PUNCT
eurjchem-1251	88	8	h	h	NOUN
eurjchem-1251	88	9	,	,	PUNCT
eurjchem-1251	88	10	4.88	4.88	NUM
eurjchem-1251	88	11	;	;	PUNCT
eurjchem-1251	88	12	n	n	CCONJ
eurjchem-1251	88	13	,	,	PUNCT
eurjchem-1251	88	14	11.96	11.96	NUM
eurjchem-1251	88	15	.	.	PUNCT
eurjchem-1251	88	16	found	find	VERB
eurjchem-1251	88	17	:	:	PUNCT
eurjchem-1251	89	1	c	c	X
eurjchem-1251	89	2	,	,	PUNCT
eurjchem-1251	89	3	78.30	78.30	NUM
eurjchem-1251	89	4	;	;	PUNCT
eurjchem-1251	89	5	h	h	NOUN
eurjchem-1251	89	6	5.00	5.00	NUM
eurjchem-1251	89	7	;	;	PUNCT
eurjchem-1251	89	8	n	n	DET
eurjchem-1251	89	9	12.20	12.20	NUM
eurjchem-1251	89	10	%	%	NOUN
eurjchem-1251	89	11	.	.	PUNCT
eurjchem-1251	90	1	deeb	deeb	PROPN
eurjchem-1251	90	2	et	et	PROPN
eurjchem-1251	90	3	al	al	PROPN
eurjchem-1251	90	4	.	.	PUNCT
eurjchem-1251	90	5	/	/	SYM
eurjchem-1251	90	6	european	european	PROPN
eurjchem-1251	90	7	journal	journal	PROPN
eurjchem-1251	90	8	of	of	ADP
eurjchem-1251	90	9	chemistry	chemistry	NOUN
eurjchem-1251	90	10	6	6	NUM
eurjchem-1251	90	11	(	(	PUNCT
eurjchem-1251	90	12	2	2	NUM
eurjchem-1251	90	13	)	)	PUNCT
eurjchem-1251	90	14	(	(	PUNCT
eurjchem-1251	90	15	2015	2015	NUM
eurjchem-1251	90	16	)	)	PUNCT
eurjchem-1251	90	17	211‐218	211‐218	NOUN
eurjchem-1251	90	18	213	213	NUM
eurjchem-1251	90	19	scheme	scheme	NOUN
eurjchem-1251	90	20	2	2	NUM
eurjchem-1251	90	21	2.2.7	2.2.7	NUM
eurjchem-1251	90	22	.	.	PUNCT
eurjchem-1251	91	1	synthesis	synthesis	NOUN
eurjchem-1251	91	2	of	of	ADP
eurjchem-1251	91	3	n‐(4,5,6‐triphenylpyridazin‐3‐yl	n‐(4,5,6‐triphenylpyridazin‐3‐yl	PROPN
eurjchem-1251	91	4	)	)	PUNCT
eurjchem-1251	91	5	acetamide	acetamide	NOUN
eurjchem-1251	91	6	(	(	PUNCT
eurjchem-1251	91	7	6b	6b	NOUN
eurjchem-1251	91	8	)	)	PUNCT
eurjchem-1251	91	9	a	a	DET
eurjchem-1251	91	10	solution	solution	NOUN
eurjchem-1251	91	11	of	of	ADP
eurjchem-1251	91	12	compound	compound	NOUN
eurjchem-1251	91	13	5	5	NUM
eurjchem-1251	91	14	(	(	PUNCT
eurjchem-1251	91	15	0.5	0.5	NUM
eurjchem-1251	91	16	g	g	NOUN
eurjchem-1251	91	17	,	,	PUNCT
eurjchem-1251	91	18	1.55	1.55	NUM
eurjchem-1251	91	19	mmol	mmol	NOUN
eurjchem-1251	91	20	)	)	PUNCT
eurjchem-1251	91	21	in	in	ADP
eurjchem-1251	91	22	acetic	acetic	ADJ
eurjchem-1251	91	23	anhydride	anhydride	NOUN
eurjchem-1251	91	24	(	(	PUNCT
eurjchem-1251	91	25	10	10	NUM
eurjchem-1251	91	26	ml	ml	NOUN
eurjchem-1251	91	27	)	)	PUNCT
eurjchem-1251	91	28	was	be	AUX
eurjchem-1251	91	29	heated	heat	VERB
eurjchem-1251	91	30	under	under	ADP
eurjchem-1251	91	31	reflux	reflux	NOUN
eurjchem-1251	91	32	for	for	ADP
eurjchem-1251	91	33	5	5	NUM
eurjchem-1251	91	34	h.	h.	NOUN
eurjchem-1251	91	35	the	the	DET
eurjchem-1251	91	36	solvent	solvent	NOUN
eurjchem-1251	91	37	was	be	AUX
eurjchem-1251	91	38	evaporated	evaporate	VERB
eurjchem-1251	91	39	under	under	ADP
eurjchem-1251	91	40	reduced	reduced	ADJ
eurjchem-1251	91	41	pressure	pressure	NOUN
eurjchem-1251	91	42	;	;	PUNCT
eurjchem-1251	91	43	the	the	DET
eurjchem-1251	91	44	solid	solid	ADJ
eurjchem-1251	91	45	residue	residue	NOUN
eurjchem-1251	91	46	was	be	AUX
eurjchem-1251	91	47	collected	collect	VERB
eurjchem-1251	91	48	and	and	CCONJ
eurjchem-1251	91	49	recrystallized	recrystallize	VERB
eurjchem-1251	91	50	from	from	ADP
eurjchem-1251	91	51	ethanol	ethanol	NOUN
eurjchem-1251	91	52	(	(	PUNCT
eurjchem-1251	91	53	scheme	scheme	NOUN
eurjchem-1251	91	54	2	2	NUM
eurjchem-1251	91	55	)	)	PUNCT
eurjchem-1251	91	56	.	.	PUNCT
eurjchem-1251	92	1	color	color	NOUN
eurjchem-1251	92	2	:	:	PUNCT
eurjchem-1251	92	3	white	white	ADJ
eurjchem-1251	92	4	.	.	PUNCT
eurjchem-1251	93	1	yield	yield	NOUN
eurjchem-1251	93	2	:	:	PUNCT
eurjchem-1251	93	3	90.26	90.26	NUM
eurjchem-1251	93	4	%	%	NOUN
eurjchem-1251	93	5	.	.	PUNCT
eurjchem-1251	94	1	m.p	m.p	PROPN
eurjchem-1251	94	2	.	.	PROPN
eurjchem-1251	94	3	:	:	PUNCT
eurjchem-1251	95	1	206‐208	206‐208	NUM
eurjchem-1251	95	2	°	°	PROPN
eurjchem-1251	95	3	c	c	X
eurjchem-1251	95	4	.	.	PUNCT
eurjchem-1251	96	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	96	2	(	(	PUNCT
eurjchem-1251	96	3	kbr	kbr	PROPN
eurjchem-1251	96	4	,	,	PUNCT
eurjchem-1251	96	5	ν	ν	PROPN
eurjchem-1251	96	6	,	,	PUNCT
eurjchem-1251	96	7	cm‐1	cm‐1	PROPN
eurjchem-1251	96	8	):	):	PUNCT
eurjchem-1251	96	9	3425	3425	NUM
eurjchem-1251	96	10	(	(	PUNCT
eurjchem-1251	96	11	nh	nh	NOUN
eurjchem-1251	96	12	)	)	PUNCT
eurjchem-1251	96	13	,	,	PUNCT
eurjchem-1251	96	14	3027(ch	3027(ch	NUM
eurjchem-1251	96	15	arom	arom	NOUN
eurjchem-1251	96	16	.	.	PUNCT
eurjchem-1251	96	17	)	)	PUNCT
eurjchem-1251	96	18	,	,	PUNCT
eurjchem-1251	96	19	2935	2935	NUM
eurjchem-1251	96	20	(	(	PUNCT
eurjchem-1251	96	21	ch	ch	NOUN
eurjchem-1251	96	22	aliph	aliph	PROPN
eurjchem-1251	96	23	.	.	PUNCT
eurjchem-1251	96	24	)	)	PUNCT
eurjchem-1251	96	25	,	,	PUNCT
eurjchem-1251	96	26	1723	1723	NUM
eurjchem-1251	96	27	(	(	PUNCT
eurjchem-1251	96	28	c	c	NOUN
eurjchem-1251	96	29	=	=	NOUN
eurjchem-1251	96	30	o	o	NOUN
eurjchem-1251	96	31	)	)	PUNCT
eurjchem-1251	96	32	,	,	PUNCT
eurjchem-1251	96	33	1629	1629	NUM
eurjchem-1251	96	34	(	(	PUNCT
eurjchem-1251	96	35	c	c	NOUN
eurjchem-1251	96	36	=	=	SYM
eurjchem-1251	96	37	n	n	NUM
eurjchem-1251	96	38	)	)	PUNCT
eurjchem-1251	96	39	.	.	PUNCT
eurjchem-1251	97	1	1h	1h	NUM
eurjchem-1251	97	2	nmr	nmr	NOUN
eurjchem-1251	97	3	(	(	PUNCT
eurjchem-1251	97	4	300	300	NUM
eurjchem-1251	97	5	mhz	mhz	NOUN
eurjchem-1251	97	6	,	,	PUNCT
eurjchem-1251	97	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	97	8	,	,	PUNCT
eurjchem-1251	97	9	δ	δ	PROPN
eurjchem-1251	97	10	,	,	PUNCT
eurjchem-1251	97	11	ppm	ppm	NUM
eurjchem-1251	97	12	):	):	PUNCT
eurjchem-1251	97	13	2.15	2.15	NUM
eurjchem-1251	97	14	(	(	PUNCT
eurjchem-1251	97	15	s	s	PROPN
eurjchem-1251	97	16	,	,	PUNCT
eurjchem-1251	97	17	3h	3h	NUM
eurjchem-1251	97	18	,	,	PUNCT
eurjchem-1251	97	19	ch3	ch3	PROPN
eurjchem-1251	97	20	)	)	PUNCT
eurjchem-1251	97	21	,	,	PUNCT
eurjchem-1251	97	22	7.02‐7.39	7.02‐7.39	NUM
eurjchem-1251	97	23	(	(	PUNCT
eurjchem-1251	97	24	m	m	PROPN
eurjchem-1251	97	25	,	,	PUNCT
eurjchem-1251	97	26	15h	15h	NUM
eurjchem-1251	97	27	,	,	PUNCT
eurjchem-1251	97	28	3ph	3ph	NOUN
eurjchem-1251	97	29	)	)	PUNCT
eurjchem-1251	97	30	,	,	PUNCT
eurjchem-1251	97	31	7.40	7.40	NUM
eurjchem-1251	97	32	(	(	PUNCT
eurjchem-1251	97	33	s	s	PROPN
eurjchem-1251	97	34	,	,	PUNCT
eurjchem-1251	97	35	1h	1h	NUM
eurjchem-1251	97	36	,	,	PUNCT
eurjchem-1251	97	37	nh	nh	PROPN
eurjchem-1251	97	38	)	)	PUNCT
eurjchem-1251	97	39	.	.	PUNCT
eurjchem-1251	98	1	ms	ms	NOUN
eurjchem-1251	98	2	(	(	PUNCT
eurjchem-1251	98	3	ei	ei	PROPN
eurjchem-1251	98	4	,	,	PUNCT
eurjchem-1251	98	5	m	m	NOUN
eurjchem-1251	98	6	/	/	SYM
eurjchem-1251	98	7	z(%	z(%	NOUN
eurjchem-1251	98	8	)	)	PUNCT
eurjchem-1251	98	9	):	):	PUNCT
eurjchem-1251	98	10	365	365	NUM
eurjchem-1251	98	11	(	(	PUNCT
eurjchem-1251	98	12	[	[	X
eurjchem-1251	98	13	m]+	m]+	NOUN
eurjchem-1251	98	14	,	,	PUNCT
eurjchem-1251	98	15	71.47	71.47	NUM
eurjchem-1251	98	16	)	)	PUNCT
eurjchem-1251	98	17	,	,	PUNCT
eurjchem-1251	98	18	364	364	NUM
eurjchem-1251	98	19	(	(	PUNCT
eurjchem-1251	98	20	[	[	X
eurjchem-1251	98	21	m‐1]+	m‐1]+	ADJ
eurjchem-1251	98	22	,	,	PUNCT
eurjchem-1251	98	23	100	100	NUM
eurjchem-1251	98	24	)	)	PUNCT
eurjchem-1251	98	25	,	,	PUNCT
eurjchem-1251	98	26	350	350	NUM
eurjchem-1251	98	27	(	(	PUNCT
eurjchem-1251	98	28	66.80	66.80	NUM
eurjchem-1251	98	29	)	)	PUNCT
eurjchem-1251	98	30	,	,	PUNCT
eurjchem-1251	98	31	322	322	NUM
eurjchem-1251	98	32	(	(	PUNCT
eurjchem-1251	98	33	61.66	61.66	NUM
eurjchem-1251	98	34	)	)	PUNCT
eurjchem-1251	98	35	,	,	PUNCT
eurjchem-1251	98	36	307	307	NUM
eurjchem-1251	98	37	(	(	PUNCT
eurjchem-1251	98	38	4.84	4.84	NUM
eurjchem-1251	98	39	)	)	PUNCT
eurjchem-1251	98	40	,	,	PUNCT
eurjchem-1251	98	41	288	288	NUM
eurjchem-1251	98	42	(	(	PUNCT
eurjchem-1251	98	43	7.68	7.68	NUM
eurjchem-1251	98	44	)	)	PUNCT
eurjchem-1251	98	45	,	,	PUNCT
eurjchem-1251	98	46	263	263	NUM
eurjchem-1251	98	47	(	(	PUNCT
eurjchem-1251	98	48	6.65	6.65	NUM
eurjchem-1251	98	49	)	)	PUNCT
eurjchem-1251	98	50	.	.	PUNCT
eurjchem-1251	99	1	anal	anal	PROPN
eurjchem-1251	99	2	.	.	PUNCT
eurjchem-1251	99	3	calcd	calcd	NOUN
eurjchem-1251	99	4	.	.	PUNCT
eurjchem-1251	100	1	for	for	ADP
eurjchem-1251	100	2	c24h19n3o	c24h19n3o	PROPN
eurjchem-1251	100	3	:	:	PUNCT
eurjchem-1251	100	4	c	c	X
eurjchem-1251	100	5	,	,	PUNCT
eurjchem-1251	100	6	78.88	78.88	NUM
eurjchem-1251	100	7	;	;	PUNCT
eurjchem-1251	100	8	h	h	NOUN
eurjchem-1251	100	9	,	,	PUNCT
eurjchem-1251	100	10	5.24	5.24	NUM
eurjchem-1251	100	11	;	;	PUNCT
eurjchem-1251	100	12	n	n	CCONJ
eurjchem-1251	100	13	,	,	PUNCT
eurjchem-1251	100	14	11.50	11.50	NUM
eurjchem-1251	100	15	.	.	PUNCT
eurjchem-1251	100	16	found	find	VERB
eurjchem-1251	100	17	:	:	PUNCT
eurjchem-1251	101	1	c	c	X
eurjchem-1251	101	2	,	,	PUNCT
eurjchem-1251	101	3	79.10	79.10	NUM
eurjchem-1251	101	4	;	;	PUNCT
eurjchem-1251	101	5	h	h	NOUN
eurjchem-1251	101	6	5.10	5.10	NUM
eurjchem-1251	101	7	;	;	PUNCT
eurjchem-1251	101	8	n	n	DET
eurjchem-1251	101	9	11.20	11.20	NUM
eurjchem-1251	101	10	%	%	NOUN
eurjchem-1251	101	11	.	.	PUNCT
eurjchem-1251	102	1	2.2.8	2.2.8	X
eurjchem-1251	102	2	.	.	PUNCT
eurjchem-1251	103	1	synthesis	synthesis	NOUN
eurjchem-1251	103	2	of	of	ADP
eurjchem-1251	103	3	n‐(4,5,6‐triphenylpyridazin‐3‐yl	n‐(4,5,6‐triphenylpyridazin‐3‐yl	NOUN
eurjchem-1251	103	4	)	)	PUNCT
eurjchem-1251	103	5	benzamide	benzamide	NOUN
eurjchem-1251	103	6	(	(	PUNCT
eurjchem-1251	103	7	6c	6c	NOUN
eurjchem-1251	103	8	)	)	PUNCT
eurjchem-1251	103	9	a	a	DET
eurjchem-1251	103	10	mixture	mixture	NOUN
eurjchem-1251	103	11	of	of	ADP
eurjchem-1251	103	12	compound	compound	NOUN
eurjchem-1251	103	13	5	5	NUM
eurjchem-1251	103	14	(	(	PUNCT
eurjchem-1251	103	15	0.5	0.5	NUM
eurjchem-1251	103	16	g	g	NOUN
eurjchem-1251	103	17	,	,	PUNCT
eurjchem-1251	103	18	1.55	1.55	NUM
eurjchem-1251	103	19	mmol	mmol	NOUN
eurjchem-1251	103	20	)	)	PUNCT
eurjchem-1251	103	21	and	and	CCONJ
eurjchem-1251	103	22	benzoyl	benzoyl	ADJ
eurjchem-1251	103	23	chloride	chloride	NOUN
eurjchem-1251	103	24	(	(	PUNCT
eurjchem-1251	103	25	0.18	0.18	NUM
eurjchem-1251	103	26	ml	ml	NOUN
eurjchem-1251	103	27	,	,	PUNCT
eurjchem-1251	103	28	1.55	1.55	NUM
eurjchem-1251	103	29	mmol	mmol	NOUN
eurjchem-1251	103	30	)	)	PUNCT
eurjchem-1251	103	31	in	in	ADP
eurjchem-1251	103	32	pyridine	pyridine	NOUN
eurjchem-1251	103	33	(	(	PUNCT
eurjchem-1251	103	34	10	10	NUM
eurjchem-1251	103	35	ml	ml	NOUN
eurjchem-1251	103	36	)	)	PUNCT
eurjchem-1251	103	37	was	be	AUX
eurjchem-1251	103	38	refluxed	refluxe	VERB
eurjchem-1251	103	39	for	for	ADP
eurjchem-1251	103	40	7	7	NUM
eurjchem-1251	103	41	h.	h.	NOUN
eurjchem-1251	103	42	after	after	ADP
eurjchem-1251	103	43	cooling	cool	VERB
eurjchem-1251	103	44	,	,	PUNCT
eurjchem-1251	103	45	the	the	DET
eurjchem-1251	103	46	reaction	reaction	NOUN
eurjchem-1251	103	47	mixture	mixture	NOUN
eurjchem-1251	103	48	was	be	AUX
eurjchem-1251	103	49	poured	pour	VERB
eurjchem-1251	103	50	into	into	ADP
eurjchem-1251	103	51	ice	ice	NOUN
eurjchem-1251	103	52	water	water	NOUN
eurjchem-1251	103	53	(	(	PUNCT
eurjchem-1251	103	54	100	100	NUM
eurjchem-1251	103	55	ml	ml	NOUN
eurjchem-1251	103	56	)	)	PUNCT
eurjchem-1251	103	57	,	,	PUNCT
eurjchem-1251	103	58	the	the	DET
eurjchem-1251	103	59	precipitate	precipitate	NOUN
eurjchem-1251	103	60	that	that	PRON
eurjchem-1251	103	61	formed	form	VERB
eurjchem-1251	103	62	was	be	AUX
eurjchem-1251	103	63	filtered	filter	VERB
eurjchem-1251	103	64	off	off	ADP
eurjchem-1251	103	65	,	,	PUNCT
eurjchem-1251	103	66	washed	wash	VERB
eurjchem-1251	103	67	with	with	ADP
eurjchem-1251	103	68	water	water	NOUN
eurjchem-1251	103	69	,	,	PUNCT
eurjchem-1251	103	70	dried	dry	VERB
eurjchem-1251	103	71	and	and	CCONJ
eurjchem-1251	103	72	recrystallized	recrystallize	VERB
eurjchem-1251	103	73	from	from	ADP
eurjchem-1251	103	74	ethanol	ethanol	NOUN
eurjchem-1251	103	75	(	(	PUNCT
eurjchem-1251	103	76	scheme	scheme	NOUN
eurjchem-1251	103	77	2	2	NUM
eurjchem-1251	103	78	)	)	PUNCT
eurjchem-1251	103	79	.	.	PUNCT
eurjchem-1251	104	1	color	color	NOUN
eurjchem-1251	104	2	:	:	PUNCT
eurjchem-1251	104	3	white	white	ADJ
eurjchem-1251	104	4	.	.	PUNCT
eurjchem-1251	105	1	yield	yield	NOUN
eurjchem-1251	105	2	:	:	PUNCT
eurjchem-1251	105	3	74.13	74.13	NUM
eurjchem-1251	105	4	%	%	NOUN
eurjchem-1251	105	5	.	.	PUNCT
eurjchem-1251	106	1	m.p	m.p	PROPN
eurjchem-1251	106	2	.	.	PROPN
eurjchem-1251	106	3	:	:	PUNCT
eurjchem-1251	107	1	227‐229	227‐229	NUM
eurjchem-1251	107	2	°	°	SYM
eurjchem-1251	107	3	c	c	X
eurjchem-1251	107	4	.	.	PUNCT
eurjchem-1251	108	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	108	2	(	(	PUNCT
eurjchem-1251	108	3	kbr	kbr	PROPN
eurjchem-1251	108	4	,	,	PUNCT
eurjchem-1251	108	5	ν	ν	PROPN
eurjchem-1251	108	6	,	,	PUNCT
eurjchem-1251	108	7	cm‐1	cm‐1	PROPN
eurjchem-1251	108	8	):	):	PUNCT
eurjchem-1251	108	9	3348	3348	NUM
eurjchem-1251	108	10	(	(	PUNCT
eurjchem-1251	108	11	nh	nh	NOUN
eurjchem-1251	108	12	amide	amide	PROPN
eurjchem-1251	108	13	)	)	PUNCT
eurjchem-1251	108	14	,	,	PUNCT
eurjchem-1251	108	15	3059	3059	NUM
eurjchem-1251	108	16	,	,	PUNCT
eurjchem-1251	108	17	3031	3031	NUM
eurjchem-1251	108	18	(	(	PUNCT
eurjchem-1251	108	19	ch‐arom	ch‐arom	PROPN
eurjchem-1251	108	20	.	.	PUNCT
eurjchem-1251	108	21	)	)	PUNCT
eurjchem-1251	108	22	,	,	PUNCT
eurjchem-1251	108	23	1704	1704	NUM
eurjchem-1251	108	24	(	(	PUNCT
eurjchem-1251	108	25	c	c	NOUN
eurjchem-1251	108	26	=	=	NOUN
eurjchem-1251	108	27	o	o	NOUN
eurjchem-1251	108	28	)	)	PUNCT
eurjchem-1251	108	29	.	.	PUNCT
eurjchem-1251	109	1	1h	1h	NUM
eurjchem-1251	109	2	nmr	nmr	NOUN
eurjchem-1251	109	3	(	(	PUNCT
eurjchem-1251	109	4	300	300	NUM
eurjchem-1251	109	5	mhz	mhz	NOUN
eurjchem-1251	109	6	,	,	PUNCT
eurjchem-1251	109	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	109	8	,	,	PUNCT
eurjchem-1251	109	9	δ	δ	PROPN
eurjchem-1251	109	10	,	,	PUNCT
eurjchem-1251	109	11	ppm	ppm	NOUN
eurjchem-1251	109	12	):	):	PUNCT
eurjchem-1251	109	13	7.13‐7.33	7.13‐7.33	NUM
eurjchem-1251	109	14	(	(	PUNCT
eurjchem-1251	109	15	m	m	PROPN
eurjchem-1251	109	16	,	,	PUNCT
eurjchem-1251	109	17	20h	20h	NOUN
eurjchem-1251	109	18	,	,	PUNCT
eurjchem-1251	109	19	4ph	4ph	NOUN
eurjchem-1251	109	20	)	)	PUNCT
eurjchem-1251	109	21	,	,	PUNCT
eurjchem-1251	109	22	7.35	7.35	NUM
eurjchem-1251	109	23	(	(	PUNCT
eurjchem-1251	109	24	s	s	PROPN
eurjchem-1251	109	25	,	,	PUNCT
eurjchem-1251	109	26	1h	1h	NUM
eurjchem-1251	109	27	,	,	PUNCT
eurjchem-1251	109	28	nh	nh	PROPN
eurjchem-1251	109	29	)	)	PUNCT
eurjchem-1251	109	30	.	.	PUNCT
eurjchem-1251	110	1	anal	anal	PROPN
eurjchem-1251	110	2	.	.	PUNCT
eurjchem-1251	110	3	calcd	calcd	NOUN
eurjchem-1251	110	4	.	.	PUNCT
eurjchem-1251	111	1	for	for	ADP
eurjchem-1251	111	2	c29h21n3o	c29h21n3o	NOUN
eurjchem-1251	111	3	:	:	PUNCT
eurjchem-1251	111	4	c	c	X
eurjchem-1251	111	5	,	,	PUNCT
eurjchem-1251	111	6	81.48	81.48	NUM
eurjchem-1251	111	7	;	;	PUNCT
eurjchem-1251	111	8	h	h	NOUN
eurjchem-1251	111	9	4.95	4.95	NUM
eurjchem-1251	111	10	;	;	PUNCT
eurjchem-1251	111	11	n	n	CCONJ
eurjchem-1251	111	12	,	,	PUNCT
eurjchem-1251	111	13	9.83	9.83	NUM
eurjchem-1251	111	14	.	.	PUNCT
eurjchem-1251	111	15	found	find	VERB
eurjchem-1251	111	16	:	:	PUNCT
eurjchem-1251	111	17	c	c	PROPN
eurjchem-1251	111	18	81.70	81.70	NUM
eurjchem-1251	111	19	;	;	PUNCT
eurjchem-1251	111	20	h	h	NOUN
eurjchem-1251	111	21	4.50	4.50	NUM
eurjchem-1251	111	22	;	;	PUNCT
eurjchem-1251	111	23	n	n	DET
eurjchem-1251	111	24	10.10	10.10	NUM
eurjchem-1251	111	25	%	%	NOUN
eurjchem-1251	111	26	.	.	PUNCT
eurjchem-1251	112	1	2.2.9	2.2.9	X
eurjchem-1251	112	2	.	.	PUNCT
eurjchem-1251	113	1	synthesis	synthesis	NOUN
eurjchem-1251	113	2	of	of	ADP
eurjchem-1251	113	3	2‐chloro‐n‐(4,5,6‐triphenylpyridazin‐3‐	2‐chloro‐n‐(4,5,6‐triphenylpyridazin‐3‐	NUM
eurjchem-1251	113	4	yl)acetamide	yl)acetamide	NOUN
eurjchem-1251	113	5	(	(	PUNCT
eurjchem-1251	113	6	6d	6d	NUM
eurjchem-1251	113	7	)	)	PUNCT
eurjchem-1251	113	8	chloroacetyl	chloroacetyl	NOUN
eurjchem-1251	113	9	chloride	chloride	NOUN
eurjchem-1251	113	10	(	(	PUNCT
eurjchem-1251	113	11	0.12	0.12	NUM
eurjchem-1251	113	12	ml	ml	NOUN
eurjchem-1251	113	13	,	,	PUNCT
eurjchem-1251	113	14	1.55	1.55	NUM
eurjchem-1251	113	15	mmol	mmol	NOUN
eurjchem-1251	113	16	)	)	PUNCT
eurjchem-1251	113	17	was	be	AUX
eurjchem-1251	113	18	added	add	VERB
eurjchem-1251	113	19	to	to	ADP
eurjchem-1251	113	20	a	a	DET
eurjchem-1251	113	21	solution	solution	NOUN
eurjchem-1251	113	22	of	of	ADP
eurjchem-1251	113	23	compound	compound	NOUN
eurjchem-1251	113	24	5	5	NUM
eurjchem-1251	113	25	(	(	PUNCT
eurjchem-1251	113	26	0.5	0.5	NUM
eurjchem-1251	113	27	g	g	NOUN
eurjchem-1251	113	28	,	,	PUNCT
eurjchem-1251	113	29	1.55	1.55	NUM
eurjchem-1251	113	30	mmol	mmol	NOUN
eurjchem-1251	113	31	)	)	PUNCT
eurjchem-1251	113	32	in	in	ADP
eurjchem-1251	113	33	pyridine	pyridine	NOUN
eurjchem-1251	113	34	(	(	PUNCT
eurjchem-1251	113	35	10	10	NUM
eurjchem-1251	113	36	ml	ml	NOUN
eurjchem-1251	113	37	)	)	PUNCT
eurjchem-1251	113	38	.	.	PUNCT
eurjchem-1251	114	1	the	the	DET
eurjchem-1251	114	2	reaction	reaction	NOUN
eurjchem-1251	114	3	mixture	mixture	NOUN
eurjchem-1251	114	4	was	be	AUX
eurjchem-1251	114	5	stirred	stir	VERB
eurjchem-1251	114	6	at	at	ADP
eurjchem-1251	114	7	room	room	NOUN
eurjchem-1251	114	8	temperature	temperature	NOUN
eurjchem-1251	114	9	for	for	ADP
eurjchem-1251	114	10	2	2	NUM
eurjchem-1251	114	11	h	h	NOUN
eurjchem-1251	114	12	,	,	PUNCT
eurjchem-1251	114	13	poured	pour	VERB
eurjchem-1251	114	14	into	into	ADP
eurjchem-1251	114	15	water	water	NOUN
eurjchem-1251	114	16	(	(	PUNCT
eurjchem-1251	114	17	100	100	NUM
eurjchem-1251	114	18	ml	ml	NOUN
eurjchem-1251	114	19	)	)	PUNCT
eurjchem-1251	114	20	;	;	PUNCT
eurjchem-1251	114	21	the	the	DET
eurjchem-1251	114	22	solid	solid	ADJ
eurjchem-1251	114	23	product	product	NOUN
eurjchem-1251	114	24	that	that	PRON
eurjchem-1251	114	25	formed	form	VERB
eurjchem-1251	114	26	was	be	AUX
eurjchem-1251	114	27	filtered	filter	VERB
eurjchem-1251	114	28	off	off	ADP
eurjchem-1251	114	29	,	,	PUNCT
eurjchem-1251	114	30	washed	wash	VERB
eurjchem-1251	114	31	with	with	ADP
eurjchem-1251	114	32	water	water	NOUN
eurjchem-1251	114	33	,	,	PUNCT
eurjchem-1251	114	34	dried	dry	VERB
eurjchem-1251	114	35	and	and	CCONJ
eurjchem-1251	114	36	recrystallized	recrystallize	VERB
eurjchem-1251	114	37	from	from	ADP
eurjchem-1251	114	38	ethanol	ethanol	NOUN
eurjchem-1251	114	39	(	(	PUNCT
eurjchem-1251	114	40	scheme	scheme	NOUN
eurjchem-1251	114	41	2	2	NUM
eurjchem-1251	114	42	)	)	PUNCT
eurjchem-1251	114	43	.	.	PUNCT
eurjchem-1251	115	1	color	color	NOUN
eurjchem-1251	115	2	:	:	PUNCT
eurjchem-1251	115	3	white	white	ADJ
eurjchem-1251	115	4	.	.	PUNCT
eurjchem-1251	116	1	yield	yield	NOUN
eurjchem-1251	116	2	:	:	PUNCT
eurjchem-1251	116	3	79.26	79.26	NUM
eurjchem-1251	116	4	%	%	NOUN
eurjchem-1251	116	5	.	.	PUNCT
eurjchem-1251	117	1	m.p	m.p	PROPN
eurjchem-1251	117	2	.	.	PROPN
eurjchem-1251	117	3	:	:	PUNCT
eurjchem-1251	118	1	272‐274	272‐274	NUM
eurjchem-1251	118	2	°	°	SYM
eurjchem-1251	118	3	c	c	X
eurjchem-1251	118	4	.	.	PUNCT
eurjchem-1251	119	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	119	2	(	(	PUNCT
eurjchem-1251	119	3	kbr	kbr	PROPN
eurjchem-1251	119	4	,	,	PUNCT
eurjchem-1251	119	5	ν	ν	PROPN
eurjchem-1251	119	6	,	,	PUNCT
eurjchem-1251	119	7	cm‐1	cm‐1	PROPN
eurjchem-1251	119	8	):	):	PUNCT
eurjchem-1251	119	9	3284	3284	NUM
eurjchem-1251	119	10	(	(	PUNCT
eurjchem-1251	119	11	nh	nh	NOUN
eurjchem-1251	119	12	amide	amide	PROPN
eurjchem-1251	119	13	)	)	PUNCT
eurjchem-1251	119	14	,	,	PUNCT
eurjchem-1251	119	15	3058	3058	NUM
eurjchem-1251	119	16	(	(	PUNCT
eurjchem-1251	119	17	ch‐arom	ch‐arom	PROPN
eurjchem-1251	119	18	.	.	PUNCT
eurjchem-1251	119	19	)	)	PUNCT
eurjchem-1251	119	20	,	,	PUNCT
eurjchem-1251	119	21	1646	1646	NUM
eurjchem-1251	119	22	(	(	PUNCT
eurjchem-1251	119	23	c	c	NOUN
eurjchem-1251	119	24	=	=	NOUN
eurjchem-1251	119	25	o	o	NOUN
eurjchem-1251	119	26	amide	amide	NOUN
eurjchem-1251	119	27	)	)	PUNCT
eurjchem-1251	119	28	.	.	PUNCT
eurjchem-1251	120	1	1h	1h	NUM
eurjchem-1251	120	2	nmr	nmr	NOUN
eurjchem-1251	120	3	(	(	PUNCT
eurjchem-1251	120	4	300	300	NUM
eurjchem-1251	120	5	mhz	mhz	NOUN
eurjchem-1251	120	6	,	,	PUNCT
eurjchem-1251	120	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	120	8	,	,	PUNCT
eurjchem-1251	120	9	δ	δ	PROPN
eurjchem-1251	120	10	,	,	PUNCT
eurjchem-1251	120	11	ppm	ppm	NUM
eurjchem-1251	120	12	):	):	PUNCT
eurjchem-1251	120	13	4.20	4.20	NUM
eurjchem-1251	120	14	(	(	PUNCT
eurjchem-1251	120	15	s	s	PROPN
eurjchem-1251	120	16	,	,	PUNCT
eurjchem-1251	120	17	2h	2h	NUM
eurjchem-1251	120	18	,	,	PUNCT
eurjchem-1251	120	19	ch2	ch2	PROPN
eurjchem-1251	120	20	)	)	PUNCT
eurjchem-1251	120	21	,	,	PUNCT
eurjchem-1251	120	22	6.93‐7.68	6.93‐7.68	NUM
eurjchem-1251	120	23	(	(	PUNCT
eurjchem-1251	120	24	m	m	PROPN
eurjchem-1251	120	25	,	,	PUNCT
eurjchem-1251	120	26	15h	15h	NUM
eurjchem-1251	120	27	,	,	PUNCT
eurjchem-1251	120	28	3ph	3ph	NOUN
eurjchem-1251	120	29	)	)	PUNCT
eurjchem-1251	120	30	,	,	PUNCT
eurjchem-1251	120	31	7.88	7.88	NUM
eurjchem-1251	120	32	(	(	PUNCT
eurjchem-1251	120	33	s	s	PROPN
eurjchem-1251	120	34	,	,	PUNCT
eurjchem-1251	120	35	1h	1h	NUM
eurjchem-1251	120	36	,	,	PUNCT
eurjchem-1251	120	37	nh	nh	PROPN
eurjchem-1251	120	38	)	)	PUNCT
eurjchem-1251	120	39	.	.	PUNCT
eurjchem-1251	121	1	anal	anal	PROPN
eurjchem-1251	121	2	.	.	PUNCT
eurjchem-1251	121	3	calcd	calcd	NOUN
eurjchem-1251	121	4	.	.	PUNCT
eurjchem-1251	122	1	for	for	SCONJ
eurjchem-1251	122	2	c24h18cln3o	c24h18cln3o	NOUN
eurjchem-1251	122	3	:	:	PUNCT
eurjchem-1251	122	4	c	c	X
eurjchem-1251	122	5	,	,	PUNCT
eurjchem-1251	122	6	72.09	72.09	NUM
eurjchem-1251	122	7	;	;	PUNCT
eurjchem-1251	122	8	h	h	NOUN
eurjchem-1251	122	9	,	,	PUNCT
eurjchem-1251	122	10	4.54	4.54	NUM
eurjchem-1251	122	11	;	;	PUNCT
eurjchem-1251	122	12	n	n	CCONJ
eurjchem-1251	122	13	,	,	PUNCT
eurjchem-1251	122	14	10.51	10.51	NUM
eurjchem-1251	122	15	.	.	PUNCT
eurjchem-1251	122	16	found	find	VERB
eurjchem-1251	122	17	:	:	PUNCT
eurjchem-1251	123	1	c	c	X
eurjchem-1251	123	2	,	,	PUNCT
eurjchem-1251	123	3	72.40	72.40	NUM
eurjchem-1251	123	4	;	;	PUNCT
eurjchem-1251	124	1	h	h	NOUN
eurjchem-1251	124	2	,	,	PUNCT
eurjchem-1251	124	3	4.80	4.80	NUM
eurjchem-1251	124	4	;	;	PUNCT
eurjchem-1251	124	5	n	n	CCONJ
eurjchem-1251	124	6	,	,	PUNCT
eurjchem-1251	124	7	10.00	10.00	NUM
eurjchem-1251	124	8	%	%	NOUN
eurjchem-1251	124	9	.	.	PUNCT
eurjchem-1251	125	1	2.2.10	2.2.10	NUM
eurjchem-1251	125	2	.	.	PUNCT
eurjchem-1251	126	1	synthesis	synthesis	NOUN
eurjchem-1251	126	2	of	of	ADP
eurjchem-1251	126	3	n‐ethylidene‐4,5,6‐triphenylpyridazin‐	n‐ethylidene‐4,5,6‐triphenylpyridazin‐	NOUN
eurjchem-1251	126	4	3‐amine	3‐amine	NUM
eurjchem-1251	126	5	(	(	PUNCT
eurjchem-1251	126	6	7	7	NUM
eurjchem-1251	126	7	)	)	PUNCT
eurjchem-1251	126	8	a	a	DET
eurjchem-1251	126	9	mixture	mixture	NOUN
eurjchem-1251	126	10	of	of	ADP
eurjchem-1251	126	11	compound	compound	NOUN
eurjchem-1251	126	12	5	5	NUM
eurjchem-1251	126	13	(	(	PUNCT
eurjchem-1251	126	14	0.5	0.5	NUM
eurjchem-1251	126	15	g	g	NOUN
eurjchem-1251	126	16	,	,	PUNCT
eurjchem-1251	126	17	1.55	1.55	NUM
eurjchem-1251	126	18	mmol	mmol	NOUN
eurjchem-1251	126	19	)	)	PUNCT
eurjchem-1251	126	20	and	and	CCONJ
eurjchem-1251	126	21	acetaldehyde	acetaldehyde	NOUN
eurjchem-1251	126	22	(	(	PUNCT
eurjchem-1251	126	23	0.1	0.1	NUM
eurjchem-1251	126	24	ml	ml	NOUN
eurjchem-1251	126	25	,	,	PUNCT
eurjchem-1251	126	26	1.55	1.55	NUM
eurjchem-1251	126	27	mmol	mmol	NOUN
eurjchem-1251	126	28	)	)	PUNCT
eurjchem-1251	126	29	was	be	AUX
eurjchem-1251	126	30	refluxed	refluxe	VERB
eurjchem-1251	126	31	for	for	ADP
eurjchem-1251	126	32	4	4	NUM
eurjchem-1251	126	33	h	h	NOUN
eurjchem-1251	126	34	,	,	PUNCT
eurjchem-1251	126	35	after	after	ADP
eurjchem-1251	126	36	cooling	cool	VERB
eurjchem-1251	126	37	,	,	PUNCT
eurjchem-1251	126	38	the	the	DET
eurjchem-1251	126	39	reaction	reaction	NOUN
eurjchem-1251	126	40	mixture	mixture	NOUN
eurjchem-1251	126	41	was	be	AUX
eurjchem-1251	126	42	treated	treat	VERB
eurjchem-1251	126	43	with	with	ADP
eurjchem-1251	126	44	diethyl	diethyl	NOUN
eurjchem-1251	126	45	ether	ether	NOUN
eurjchem-1251	126	46	(	(	PUNCT
eurjchem-1251	126	47	50	50	NUM
eurjchem-1251	126	48	ml	ml	NOUN
eurjchem-1251	126	49	)	)	PUNCT
eurjchem-1251	126	50	.	.	PUNCT
eurjchem-1251	127	1	the	the	DET
eurjchem-1251	127	2	solid	solid	ADJ
eurjchem-1251	127	3	product	product	NOUN
eurjchem-1251	127	4	was	be	AUX
eurjchem-1251	127	5	filtered	filter	VERB
eurjchem-1251	127	6	off	off	ADP
eurjchem-1251	127	7	,	,	PUNCT
eurjchem-1251	127	8	dried	dry	VERB
eurjchem-1251	127	9	,	,	PUNCT
eurjchem-1251	127	10	and	and	CCONJ
eurjchem-1251	127	11	recrystallized	recrystallize	VERB
eurjchem-1251	127	12	from	from	ADP
eurjchem-1251	127	13	ethanol	ethanol	NOUN
eurjchem-1251	127	14	(	(	PUNCT
eurjchem-1251	127	15	scheme	scheme	NOUN
eurjchem-1251	127	16	2	2	NUM
eurjchem-1251	127	17	)	)	PUNCT
eurjchem-1251	127	18	.	.	PUNCT
eurjchem-1251	128	1	color	color	NOUN
eurjchem-1251	128	2	:	:	PUNCT
eurjchem-1251	128	3	brown	brown	ADJ
eurjchem-1251	128	4	.	.	PUNCT
eurjchem-1251	129	1	yield	yield	NOUN
eurjchem-1251	129	2	:	:	PUNCT
eurjchem-1251	129	3	79.26	79.26	NUM
eurjchem-1251	129	4	%	%	NOUN
eurjchem-1251	129	5	.	.	PUNCT
eurjchem-1251	130	1	m.p	m.p	PROPN
eurjchem-1251	130	2	.	.	PROPN
eurjchem-1251	130	3	:	:	PUNCT
eurjchem-1251	131	1	233‐235	233‐235	NUM
eurjchem-1251	131	2	°	°	SYM
eurjchem-1251	131	3	c	c	NOUN
eurjchem-1251	131	4	.	.	PUNCT
eurjchem-1251	132	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	132	2	(	(	PUNCT
eurjchem-1251	132	3	kbr	kbr	PROPN
eurjchem-1251	132	4	,	,	PUNCT
eurjchem-1251	132	5	ν	ν	PROPN
eurjchem-1251	132	6	,	,	PUNCT
eurjchem-1251	132	7	cm‐1	cm‐1	PROPN
eurjchem-1251	132	8	):	):	PUNCT
eurjchem-1251	132	9	3056	3056	NUM
eurjchem-1251	132	10	,	,	PUNCT
eurjchem-1251	132	11	3026	3026	NUM
eurjchem-1251	132	12	(	(	PUNCT
eurjchem-1251	132	13	ch	ch	NOUN
eurjchem-1251	132	14	arom	arom	NOUN
eurjchem-1251	132	15	.	.	PUNCT
eurjchem-1251	132	16	)	)	PUNCT
eurjchem-1251	132	17	,	,	PUNCT
eurjchem-1251	132	18	2963	2963	NUM
eurjchem-1251	132	19	,	,	PUNCT
eurjchem-1251	132	20	2873	2873	NUM
eurjchem-1251	132	21	(	(	PUNCT
eurjchem-1251	132	22	ch	ch	NOUN
eurjchem-1251	132	23	aliph	aliph	PROPN
eurjchem-1251	132	24	.	.	PUNCT
eurjchem-1251	132	25	)	)	PUNCT
eurjchem-1251	132	26	,	,	PUNCT
eurjchem-1251	132	27	1690	1690	NUM
eurjchem-1251	132	28	(	(	PUNCT
eurjchem-1251	132	29	c	c	NOUN
eurjchem-1251	132	30	=	=	NOUN
eurjchem-1251	132	31	n	n	PRON
eurjchem-1251	132	32	imino	imino	NOUN
eurjchem-1251	132	33	)	)	PUNCT
eurjchem-1251	132	34	.	.	PUNCT
eurjchem-1251	133	1	1h	1h	NUM
eurjchem-1251	133	2	nmr	nmr	NOUN
eurjchem-1251	133	3	(	(	PUNCT
eurjchem-1251	133	4	300	300	NUM
eurjchem-1251	133	5	mhz	mhz	NOUN
eurjchem-1251	133	6	,	,	PUNCT
eurjchem-1251	133	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	133	8	,	,	PUNCT
eurjchem-1251	133	9	δ	δ	PROPN
eurjchem-1251	133	10	,	,	PUNCT
eurjchem-1251	133	11	ppm	ppm	NUM
eurjchem-1251	133	12	):	):	PUNCT
eurjchem-1251	133	13	1.80	1.80	NUM
eurjchem-1251	133	14	(	(	PUNCT
eurjchem-1251	133	15	d	d	PROPN
eurjchem-1251	133	16	,	,	PUNCT
eurjchem-1251	133	17	3h	3h	NUM
eurjchem-1251	133	18	,	,	PUNCT
eurjchem-1251	133	19	ch3	ch3	PROPN
eurjchem-1251	133	20	)	)	PUNCT
eurjchem-1251	133	21	,	,	PUNCT
eurjchem-1251	133	22	7.18‐7.63	7.18‐7.63	X
eurjchem-1251	133	23	(	(	PUNCT
eurjchem-1251	133	24	m	m	PROPN
eurjchem-1251	133	25	,	,	PUNCT
eurjchem-1251	133	26	16h	16h	NUM
eurjchem-1251	133	27	,	,	PUNCT
eurjchem-1251	133	28	3ph	3ph	NOUN
eurjchem-1251	133	29	,	,	PUNCT
eurjchem-1251	133	30	=	=	NOUN
eurjchem-1251	133	31	ch	ch	NOUN
eurjchem-1251	133	32	)	)	PUNCT
eurjchem-1251	133	33	.	.	PUNCT
eurjchem-1251	134	1	anal	anal	PROPN
eurjchem-1251	134	2	.	.	PUNCT
eurjchem-1251	134	3	calcd	calcd	NOUN
eurjchem-1251	134	4	.	.	PUNCT
eurjchem-1251	135	1	for	for	SCONJ
eurjchem-1251	135	2	c24h19n3	c24h19n3	NOUN
eurjchem-1251	135	3	:	:	PUNCT
eurjchem-1251	135	4	c	c	NOUN
eurjchem-1251	135	5	,	,	PUNCT
eurjchem-1251	135	6	82.49	82.49	NUM
eurjchem-1251	135	7	;	;	PUNCT
eurjchem-1251	135	8	h	h	NOUN
eurjchem-1251	135	9	,	,	PUNCT
eurjchem-1251	135	10	5.48	5.48	NUM
eurjchem-1251	135	11	;	;	PUNCT
eurjchem-1251	135	12	n	n	CCONJ
eurjchem-1251	135	13	,	,	PUNCT
eurjchem-1251	135	14	12.03	12.03	NUM
eurjchem-1251	135	15	.	.	PUNCT
eurjchem-1251	135	16	found	find	VERB
eurjchem-1251	135	17	:	:	PUNCT
eurjchem-1251	136	1	c	c	X
eurjchem-1251	136	2	,	,	PUNCT
eurjchem-1251	136	3	82.10	82.10	NUM
eurjchem-1251	136	4	;	;	PUNCT
eurjchem-1251	136	5	h	h	NOUN
eurjchem-1251	136	6	,	,	PUNCT
eurjchem-1251	136	7	5.40	5.40	NUM
eurjchem-1251	136	8	;	;	PUNCT
eurjchem-1251	136	9	n	n	CCONJ
eurjchem-1251	136	10	,	,	PUNCT
eurjchem-1251	136	11	12.3	12.3	NUM
eurjchem-1251	136	12	%	%	NOUN
eurjchem-1251	136	13	.	.	PUNCT
eurjchem-1251	137	1	2.2.11	2.2.11	X
eurjchem-1251	137	2	.	.	PUNCT
eurjchem-1251	138	1	synthesis	synthesis	NOUN
eurjchem-1251	138	2	of	of	ADP
eurjchem-1251	138	3	n	n	CCONJ
eurjchem-1251	138	4	,	,	PUNCT
eurjchem-1251	138	5	n‐bis(4,5,6‐triphenylpyridazin‐3‐yl	n‐bis(4,5,6‐triphenylpyridazin‐3‐yl	PROPN
eurjchem-1251	138	6	)	)	PUNCT
eurjchem-1251	138	7	propanediamide	propanediamide	NOUN
eurjchem-1251	138	8	(	(	PUNCT
eurjchem-1251	138	9	8)	8)	NUM
eurjchem-1251	138	10	a	a	DET
eurjchem-1251	138	11	mixture	mixture	NOUN
eurjchem-1251	138	12	of	of	ADP
eurjchem-1251	138	13	compound	compound	NOUN
eurjchem-1251	138	14	5	5	NUM
eurjchem-1251	138	15	(	(	PUNCT
eurjchem-1251	138	16	0.5	0.5	NUM
eurjchem-1251	138	17	g	g	NOUN
eurjchem-1251	138	18	,	,	PUNCT
eurjchem-1251	138	19	1.55	1.55	NUM
eurjchem-1251	138	20	mmol	mmol	NOUN
eurjchem-1251	138	21	)	)	PUNCT
eurjchem-1251	138	22	and	and	CCONJ
eurjchem-1251	138	23	diethyl	diethyl	NOUN
eurjchem-1251	138	24	malonate	malonate	NOUN
eurjchem-1251	138	25	(	(	PUNCT
eurjchem-1251	138	26	0.24	0.24	NUM
eurjchem-1251	138	27	g	g	NOUN
eurjchem-1251	138	28	,	,	PUNCT
eurjchem-1251	138	29	1.55	1.55	NUM
eurjchem-1251	138	30	mmol	mmol	NOUN
eurjchem-1251	138	31	)	)	PUNCT
eurjchem-1251	138	32	was	be	AUX
eurjchem-1251	138	33	heated	heat	VERB
eurjchem-1251	138	34	under	under	ADP
eurjchem-1251	138	35	reflux	reflux	NOUN
eurjchem-1251	138	36	for	for	ADP
eurjchem-1251	138	37	3	3	NUM
eurjchem-1251	138	38	h.	h.	NOUN
eurjchem-1251	138	39	after	after	ADP
eurjchem-1251	138	40	cooling	cool	VERB
eurjchem-1251	138	41	,	,	PUNCT
eurjchem-1251	138	42	the	the	DET
eurjchem-1251	138	43	reaction	reaction	NOUN
eurjchem-1251	138	44	mixture	mixture	NOUN
eurjchem-1251	138	45	was	be	AUX
eurjchem-1251	138	46	treated	treat	VERB
eurjchem-1251	138	47	with	with	ADP
eurjchem-1251	138	48	diethyl	diethyl	NOUN
eurjchem-1251	138	49	ether	ether	NOUN
eurjchem-1251	138	50	(	(	PUNCT
eurjchem-1251	138	51	50	50	NUM
eurjchem-1251	138	52	ml	ml	NOUN
eurjchem-1251	138	53	)	)	PUNCT
eurjchem-1251	138	54	,	,	PUNCT
eurjchem-1251	138	55	and	and	CCONJ
eurjchem-1251	138	56	the	the	DET
eurjchem-1251	138	57	solid	solid	ADJ
eurjchem-1251	138	58	product	product	NOUN
eurjchem-1251	138	59	was	be	AUX
eurjchem-1251	138	60	filtered	filter	VERB
eurjchem-1251	138	61	off	off	ADP
eurjchem-1251	138	62	,	,	PUNCT
eurjchem-1251	138	63	dried	dry	VERB
eurjchem-1251	138	64	and	and	CCONJ
eurjchem-1251	138	65	recrystallized	recrystallize	VERB
eurjchem-1251	138	66	from	from	ADP
eurjchem-1251	138	67	dimethylformamide	dimethylformamide	NOUN
eurjchem-1251	138	68	(	(	PUNCT
eurjchem-1251	138	69	scheme	scheme	NOUN
eurjchem-1251	138	70	2	2	NUM
eurjchem-1251	138	71	)	)	PUNCT
eurjchem-1251	138	72	.	.	PUNCT
eurjchem-1251	139	1	color	color	NOUN
eurjchem-1251	139	2	:	:	PUNCT
eurjchem-1251	139	3	white	white	ADJ
eurjchem-1251	139	4	.	.	PUNCT
eurjchem-1251	140	1	yield	yield	NOUN
eurjchem-1251	140	2	:	:	PUNCT
eurjchem-1251	140	3	81.43	81.43	NUM
eurjchem-1251	140	4	%	%	NOUN
eurjchem-1251	140	5	.	.	PUNCT
eurjchem-1251	141	1	m.p	m.p	PROPN
eurjchem-1251	141	2	.	.	PROPN
eurjchem-1251	141	3	:	:	PUNCT
eurjchem-1251	142	1	218‐220	218‐220	NUM
eurjchem-1251	142	2	°	°	ADP
eurjchem-1251	142	3	c	c	NOUN
eurjchem-1251	142	4	.	.	PUNCT
eurjchem-1251	142	5	ft‐ir	ft‐ir	NOUN
eurjchem-1251	142	6	(	(	PUNCT
eurjchem-1251	142	7	kbr	kbr	PROPN
eurjchem-1251	142	8	,	,	PUNCT
eurjchem-1251	142	9	ν	ν	PROPN
eurjchem-1251	142	10	,	,	PUNCT
eurjchem-1251	142	11	cm‐1	cm‐1	PROPN
eurjchem-1251	142	12	):	):	PUNCT
eurjchem-1251	142	13	3156	3156	NUM
eurjchem-1251	142	14	(	(	PUNCT
eurjchem-1251	142	15	nh	nh	NOUN
eurjchem-1251	142	16	amide	amide	NOUN
eurjchem-1251	142	17	)	)	PUNCT
eurjchem-1251	142	18	,	,	PUNCT
eurjchem-1251	142	19	3059	3059	NUM
eurjchem-1251	142	20	,	,	PUNCT
eurjchem-1251	142	21	3024	3024	NUM
eurjchem-1251	142	22	(	(	PUNCT
eurjchem-1251	142	23	ch	ch	NOUN
eurjchem-1251	142	24	arom	arom	NOUN
eurjchem-1251	142	25	.	.	PUNCT
eurjchem-1251	142	26	)	)	PUNCT
eurjchem-1251	142	27	,	,	PUNCT
eurjchem-1251	142	28	2972	2972	NUM
eurjchem-1251	142	29	,	,	PUNCT
eurjchem-1251	142	30	2816	2816	NUM
eurjchem-1251	142	31	(	(	PUNCT
eurjchem-1251	142	32	ch	ch	NOUN
eurjchem-1251	142	33	aliph	aliph	PROPN
eurjchem-1251	142	34	.	.	PUNCT
eurjchem-1251	142	35	)	)	PUNCT
eurjchem-1251	142	36	,	,	PUNCT
eurjchem-1251	142	37	1698	1698	NUM
eurjchem-1251	142	38	(	(	PUNCT
eurjchem-1251	142	39	c	c	NOUN
eurjchem-1251	142	40	=	=	NOUN
eurjchem-1251	142	41	o	o	NOUN
eurjchem-1251	142	42	amide	amide	NOUN
eurjchem-1251	142	43	)	)	PUNCT
eurjchem-1251	142	44	.	.	PUNCT
eurjchem-1251	143	1	1h	1h	NUM
eurjchem-1251	143	2	nmr	nmr	NOUN
eurjchem-1251	143	3	(	(	PUNCT
eurjchem-1251	143	4	300	300	NUM
eurjchem-1251	143	5	mhz	mhz	NOUN
eurjchem-1251	143	6	,	,	PUNCT
eurjchem-1251	143	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	143	8	,	,	PUNCT
eurjchem-1251	143	9	δ	δ	PROPN
eurjchem-1251	143	10	,	,	PUNCT
eurjchem-1251	143	11	ppm	ppm	NUM
eurjchem-1251	143	12	):	):	PUNCT
eurjchem-1251	143	13	1.80	1.80	NUM
eurjchem-1251	143	14	(	(	PUNCT
eurjchem-1251	143	15	s	s	PROPN
eurjchem-1251	143	16	,	,	PUNCT
eurjchem-1251	143	17	2h	2h	NUM
eurjchem-1251	143	18	,	,	PUNCT
eurjchem-1251	143	19	ch2	ch2	PROPN
eurjchem-1251	143	20	)	)	PUNCT
eurjchem-1251	143	21	,	,	PUNCT
eurjchem-1251	143	22	6.87‐7.31	6.87‐7.31	NUM
eurjchem-1251	143	23	(	(	PUNCT
eurjchem-1251	143	24	m	m	PROPN
eurjchem-1251	143	25	,	,	PUNCT
eurjchem-1251	143	26	30h	30h	NOUN
eurjchem-1251	143	27	,	,	PUNCT
eurjchem-1251	143	28	6ph	6ph	ADJ
eurjchem-1251	143	29	)	)	PUNCT
eurjchem-1251	143	30	,	,	PUNCT
eurjchem-1251	143	31	10.23	10.23	NUM
eurjchem-1251	143	32	(	(	PUNCT
eurjchem-1251	143	33	s	s	PROPN
eurjchem-1251	143	34	,	,	PUNCT
eurjchem-1251	143	35	2h	2h	NUM
eurjchem-1251	143	36	,	,	PUNCT
eurjchem-1251	143	37	2nh	2nh	NOUN
eurjchem-1251	143	38	)	)	PUNCT
eurjchem-1251	143	39	.	.	PUNCT
eurjchem-1251	144	1	214	214	NUM
eurjchem-1251	144	2	deeb	deeb	PROPN
eurjchem-1251	144	3	et	et	PROPN
eurjchem-1251	144	4	al	al	PROPN
eurjchem-1251	144	5	.	.	PUNCT
eurjchem-1251	144	6	/	/	SYM
eurjchem-1251	144	7	european	european	PROPN
eurjchem-1251	144	8	journal	journal	PROPN
eurjchem-1251	144	9	of	of	ADP
eurjchem-1251	144	10	chemistry	chemistry	NOUN
eurjchem-1251	144	11	6	6	NUM
eurjchem-1251	144	12	(	(	PUNCT
eurjchem-1251	144	13	2	2	NUM
eurjchem-1251	144	14	)	)	PUNCT
eurjchem-1251	144	15	(	(	PUNCT
eurjchem-1251	144	16	2015	2015	NUM
eurjchem-1251	144	17	)	)	PUNCT
eurjchem-1251	144	18	211‐218	211‐218	NUM
eurjchem-1251	144	19	scheme	scheme	NOUN
eurjchem-1251	144	20	3	3	NUM
eurjchem-1251	144	21	ms	ms	NOUN
eurjchem-1251	144	22	(	(	PUNCT
eurjchem-1251	144	23	ei	ei	PROPN
eurjchem-1251	144	24	,	,	PUNCT
eurjchem-1251	144	25	m	m	PROPN
eurjchem-1251	144	26	/	/	SYM
eurjchem-1251	144	27	z	z	PROPN
eurjchem-1251	144	28	(	(	PUNCT
eurjchem-1251	144	29	%	%	NOUN
eurjchem-1251	144	30	)	)	PUNCT
eurjchem-1251	144	31	):	):	PUNCT
eurjchem-1251	144	32	714	714	NUM
eurjchem-1251	144	33	(	(	PUNCT
eurjchem-1251	144	34	[	[	X
eurjchem-1251	144	35	m]+	m]+	NOUN
eurjchem-1251	144	36	,	,	PUNCT
eurjchem-1251	144	37	7.92	7.92	NUM
eurjchem-1251	144	38	)	)	PUNCT
eurjchem-1251	144	39	,	,	PUNCT
eurjchem-1251	144	40	658	658	NUM
eurjchem-1251	144	41	(	(	PUNCT
eurjchem-1251	144	42	9.09	9.09	NUM
eurjchem-1251	144	43	)	)	PUNCT
eurjchem-1251	144	44	,	,	PUNCT
eurjchem-1251	144	45	406	406	NUM
eurjchem-1251	144	46	(	(	PUNCT
eurjchem-1251	144	47	7.92	7.92	NUM
eurjchem-1251	144	48	)	)	PUNCT
eurjchem-1251	144	49	,	,	PUNCT
eurjchem-1251	144	50	363	363	NUM
eurjchem-1251	144	51	(	(	PUNCT
eurjchem-1251	144	52	58.50	58.50	NUM
eurjchem-1251	144	53	)	)	PUNCT
eurjchem-1251	144	54	,	,	PUNCT
eurjchem-1251	144	55	322	322	NUM
eurjchem-1251	144	56	(	(	PUNCT
eurjchem-1251	144	57	100	100	NUM
eurjchem-1251	144	58	)	)	PUNCT
eurjchem-1251	144	59	.	.	PUNCT
eurjchem-1251	145	1	anal	anal	PROPN
eurjchem-1251	145	2	.	.	PUNCT
eurjchem-1251	145	3	calcd	calcd	NOUN
eurjchem-1251	145	4	.	.	PUNCT
eurjchem-1251	146	1	for	for	ADP
eurjchem-1251	146	2	c47h34n6o2	c47h34n6o2	NOUN
eurjchem-1251	146	3	:	:	PUNCT
eurjchem-1251	146	4	c	c	X
eurjchem-1251	146	5	,	,	PUNCT
eurjchem-1251	146	6	78.97	78.97	NUM
eurjchem-1251	146	7	;	;	PUNCT
eurjchem-1251	146	8	h	h	NOUN
eurjchem-1251	146	9	,	,	PUNCT
eurjchem-1251	146	10	4.79	4.79	NUM
eurjchem-1251	146	11	;	;	PUNCT
eurjchem-1251	146	12	n	n	CCONJ
eurjchem-1251	146	13	,	,	PUNCT
eurjchem-1251	146	14	11.67	11.67	NUM
eurjchem-1251	146	15	.	.	PUNCT
eurjchem-1251	146	16	found	find	VERB
eurjchem-1251	146	17	:	:	PUNCT
eurjchem-1251	146	18	c	c	PROPN
eurjchem-1251	146	19	79.30	79.30	NUM
eurjchem-1251	146	20	;	;	PUNCT
eurjchem-1251	146	21	h	h	NOUN
eurjchem-1251	146	22	,	,	PUNCT
eurjchem-1251	146	23	4.69	4.69	NUM
eurjchem-1251	146	24	;	;	PUNCT
eurjchem-1251	146	25	n	n	CCONJ
eurjchem-1251	146	26	,	,	PUNCT
eurjchem-1251	146	27	12.00	12.00	NUM
eurjchem-1251	146	28	%	%	NOUN
eurjchem-1251	146	29	.	.	PUNCT
eurjchem-1251	147	1	2.2.12	2.2.12	X
eurjchem-1251	147	2	.	.	PUNCT
eurjchem-1251	147	3	synthesis	synthesis	NOUN
eurjchem-1251	147	4	of	of	ADP
eurjchem-1251	147	5	7,8,9‐triphenyl‐2h‐pyrimido[1,2‐b	7,8,9‐triphenyl‐2h‐pyrimido[1,2‐b	NUM
eurjchem-1251	147	6	]	]	X
eurjchem-1251	147	7	pyridazine‐2,4(3h)‐dione	pyridazine‐2,4(3h)‐dione	NUM
eurjchem-1251	147	8	(	(	PUNCT
eurjchem-1251	147	9	9	9	NUM
eurjchem-1251	147	10	)	)	PUNCT
eurjchem-1251	147	11	a	a	DET
eurjchem-1251	147	12	mixture	mixture	NOUN
eurjchem-1251	147	13	of	of	ADP
eurjchem-1251	147	14	compound	compound	NOUN
eurjchem-1251	147	15	5	5	NUM
eurjchem-1251	147	16	(	(	PUNCT
eurjchem-1251	147	17	0.5	0.5	NUM
eurjchem-1251	147	18	g	g	NOUN
eurjchem-1251	147	19	,	,	PUNCT
eurjchem-1251	147	20	1.55	1.55	NUM
eurjchem-1251	147	21	mmol	mmol	NOUN
eurjchem-1251	147	22	)	)	PUNCT
eurjchem-1251	147	23	,	,	PUNCT
eurjchem-1251	147	24	malonic	malonic	ADJ
eurjchem-1251	147	25	acid	acid	NOUN
eurjchem-1251	147	26	(	(	PUNCT
eurjchem-1251	147	27	0.16	0.16	NUM
eurjchem-1251	147	28	g	g	NOUN
eurjchem-1251	147	29	,	,	PUNCT
eurjchem-1251	147	30	1.55	1.55	NUM
eurjchem-1251	147	31	mmol	mmol	NOUN
eurjchem-1251	147	32	)	)	PUNCT
eurjchem-1251	147	33	and	and	CCONJ
eurjchem-1251	147	34	phosphoryl	phosphoryl	PROPN
eurjchem-1251	147	35	chloride	chloride	PROPN
eurjchem-1251	147	36	(	(	PUNCT
eurjchem-1251	147	37	10	10	NUM
eurjchem-1251	147	38	ml	ml	NOUN
eurjchem-1251	147	39	)	)	PUNCT
eurjchem-1251	147	40	was	be	AUX
eurjchem-1251	147	41	heated	heat	VERB
eurjchem-1251	147	42	under	under	ADP
eurjchem-1251	147	43	reflux	reflux	NOUN
eurjchem-1251	147	44	for	for	ADP
eurjchem-1251	147	45	1	1	NUM
eurjchem-1251	147	46	h.	h.	NOUN
eurjchem-1251	147	47	the	the	DET
eurjchem-1251	147	48	reaction	reaction	NOUN
eurjchem-1251	147	49	mixture	mixture	NOUN
eurjchem-1251	147	50	was	be	AUX
eurjchem-1251	147	51	cooled	cool	VERB
eurjchem-1251	147	52	to	to	ADP
eurjchem-1251	147	53	room	room	NOUN
eurjchem-1251	147	54	temperature	temperature	NOUN
eurjchem-1251	147	55	and	and	CCONJ
eurjchem-1251	147	56	poured	pour	VERB
eurjchem-1251	147	57	into	into	ADP
eurjchem-1251	147	58	ice	ice	NOUN
eurjchem-1251	147	59	cooled	cool	VERB
eurjchem-1251	147	60	water	water	NOUN
eurjchem-1251	147	61	(	(	PUNCT
eurjchem-1251	147	62	200	200	NUM
eurjchem-1251	147	63	ml	ml	NOUN
eurjchem-1251	147	64	)	)	PUNCT
eurjchem-1251	147	65	.	.	PUNCT
eurjchem-1251	148	1	the	the	DET
eurjchem-1251	148	2	solid	solid	ADJ
eurjchem-1251	148	3	product	product	NOUN
eurjchem-1251	148	4	was	be	AUX
eurjchem-1251	148	5	filtered	filter	VERB
eurjchem-1251	148	6	off	off	ADP
eurjchem-1251	148	7	,	,	PUNCT
eurjchem-1251	148	8	washed	wash	VERB
eurjchem-1251	148	9	with	with	ADP
eurjchem-1251	148	10	water	water	NOUN
eurjchem-1251	148	11	,	,	PUNCT
eurjchem-1251	148	12	dried	dry	VERB
eurjchem-1251	148	13	and	and	CCONJ
eurjchem-1251	148	14	recrystallized	recrystallize	VERB
eurjchem-1251	148	15	from	from	ADP
eurjchem-1251	148	16	ethanol	ethanol	NOUN
eurjchem-1251	148	17	(	(	PUNCT
eurjchem-1251	148	18	scheme	scheme	NOUN
eurjchem-1251	148	19	2	2	NUM
eurjchem-1251	148	20	)	)	PUNCT
eurjchem-1251	148	21	.	.	PUNCT
eurjchem-1251	149	1	color	color	NOUN
eurjchem-1251	149	2	:	:	PUNCT
eurjchem-1251	149	3	yellow	yellow	ADJ
eurjchem-1251	149	4	.	.	PUNCT
eurjchem-1251	150	1	yield	yield	NOUN
eurjchem-1251	150	2	:	:	PUNCT
eurjchem-1251	150	3	72.70	72.70	NUM
eurjchem-1251	150	4	%	%	NOUN
eurjchem-1251	150	5	.	.	PUNCT
eurjchem-1251	151	1	m.p	m.p	PROPN
eurjchem-1251	151	2	.	.	PROPN
eurjchem-1251	151	3	:	:	PUNCT
eurjchem-1251	152	1	188‐190	188‐190	NUM
eurjchem-1251	152	2	°	°	ADP
eurjchem-1251	152	3	c	c	X
eurjchem-1251	152	4	.	.	PUNCT
eurjchem-1251	153	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	153	2	(	(	PUNCT
eurjchem-1251	153	3	kbr	kbr	PROPN
eurjchem-1251	153	4	,	,	PUNCT
eurjchem-1251	153	5	ν	ν	PROPN
eurjchem-1251	153	6	,	,	PUNCT
eurjchem-1251	153	7	cm‐1	cm‐1	PROPN
eurjchem-1251	153	8	):	):	PUNCT
eurjchem-1251	153	9	3057	3057	NUM
eurjchem-1251	153	10	(	(	PUNCT
eurjchem-1251	153	11	ch	ch	NOUN
eurjchem-1251	153	12	arom	arom	NOUN
eurjchem-1251	153	13	.	.	PUNCT
eurjchem-1251	153	14	)	)	PUNCT
eurjchem-1251	153	15	,	,	PUNCT
eurjchem-1251	153	16	2923	2923	NUM
eurjchem-1251	153	17	(	(	PUNCT
eurjchem-1251	153	18	ch	ch	NOUN
eurjchem-1251	153	19	aliph	aliph	PROPN
eurjchem-1251	153	20	.	.	PUNCT
eurjchem-1251	153	21	)	)	PUNCT
eurjchem-1251	153	22	,	,	PUNCT
eurjchem-1251	153	23	1703	1703	NUM
eurjchem-1251	153	24	(	(	PUNCT
eurjchem-1251	153	25	c	c	NOUN
eurjchem-1251	153	26	=	=	NOUN
eurjchem-1251	153	27	o	o	NOUN
eurjchem-1251	153	28	)	)	PUNCT
eurjchem-1251	153	29	,	,	PUNCT
eurjchem-1251	153	30	1636	1636	NUM
eurjchem-1251	153	31	(	(	PUNCT
eurjchem-1251	153	32	c	c	NOUN
eurjchem-1251	153	33	=	=	SYM
eurjchem-1251	153	34	n	n	NUM
eurjchem-1251	153	35	)	)	PUNCT
eurjchem-1251	153	36	.	.	PUNCT
eurjchem-1251	154	1	1h	1h	NUM
eurjchem-1251	154	2	nmr	nmr	NOUN
eurjchem-1251	154	3	(	(	PUNCT
eurjchem-1251	154	4	300	300	NUM
eurjchem-1251	154	5	mhz	mhz	NOUN
eurjchem-1251	154	6	,	,	PUNCT
eurjchem-1251	154	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	154	8	,	,	PUNCT
eurjchem-1251	154	9	δ	δ	PROPN
eurjchem-1251	154	10	,	,	PUNCT
eurjchem-1251	154	11	ppm	ppm	NUM
eurjchem-1251	154	12	):	):	PUNCT
eurjchem-1251	154	13	3.99	3.99	NUM
eurjchem-1251	154	14	(	(	PUNCT
eurjchem-1251	154	15	s	s	PROPN
eurjchem-1251	154	16	,	,	PUNCT
eurjchem-1251	154	17	2h	2h	NUM
eurjchem-1251	154	18	,	,	PUNCT
eurjchem-1251	154	19	ch2	ch2	PROPN
eurjchem-1251	154	20	)	)	PUNCT
eurjchem-1251	154	21	,	,	PUNCT
eurjchem-1251	154	22	6.78‐	6.78‐	NOUN
eurjchem-1251	154	23	7.65	7.65	NUM
eurjchem-1251	154	24	(	(	PUNCT
eurjchem-1251	154	25	m	m	PROPN
eurjchem-1251	154	26	,	,	PUNCT
eurjchem-1251	154	27	15h	15h	NUM
eurjchem-1251	154	28	,	,	PUNCT
eurjchem-1251	154	29	3ph	3ph	NOUN
eurjchem-1251	154	30	)	)	PUNCT
eurjchem-1251	154	31	.	.	PUNCT
eurjchem-1251	155	1	ms	ms	NOUN
eurjchem-1251	155	2	(	(	PUNCT
eurjchem-1251	155	3	ei	ei	PROPN
eurjchem-1251	155	4	,	,	PUNCT
eurjchem-1251	155	5	m	m	PROPN
eurjchem-1251	155	6	/	/	SYM
eurjchem-1251	155	7	z	z	PROPN
eurjchem-1251	155	8	(	(	PUNCT
eurjchem-1251	155	9	%	%	NOUN
eurjchem-1251	155	10	)	)	PUNCT
eurjchem-1251	155	11	):	):	PUNCT
eurjchem-1251	155	12	391	391	NUM
eurjchem-1251	155	13	(	(	PUNCT
eurjchem-1251	155	14	m+	m+	NUM
eurjchem-1251	155	15	,	,	PUNCT
eurjchem-1251	155	16	72.07	72.07	NUM
eurjchem-1251	155	17	)	)	PUNCT
eurjchem-1251	155	18	,	,	PUNCT
eurjchem-1251	155	19	363	363	NUM
eurjchem-1251	155	20	(	(	PUNCT
eurjchem-1251	155	21	11.24	11.24	NUM
eurjchem-1251	155	22	)	)	PUNCT
eurjchem-1251	155	23	,	,	PUNCT
eurjchem-1251	155	24	349	349	NUM
eurjchem-1251	155	25	(	(	PUNCT
eurjchem-1251	155	26	10.60	10.60	NUM
eurjchem-1251	155	27	)	)	PUNCT
eurjchem-1251	155	28	,	,	PUNCT
eurjchem-1251	155	29	335	335	NUM
eurjchem-1251	155	30	(	(	PUNCT
eurjchem-1251	155	31	5.41	5.41	NUM
eurjchem-1251	155	32	)	)	PUNCT
eurjchem-1251	155	33	,	,	PUNCT
eurjchem-1251	155	34	321	321	NUM
eurjchem-1251	155	35	(	(	PUNCT
eurjchem-1251	155	36	16.82	16.82	NUM
eurjchem-1251	155	37	)	)	PUNCT
eurjchem-1251	155	38	,	,	PUNCT
eurjchem-1251	155	39	314	314	NUM
eurjchem-1251	155	40	(	(	PUNCT
eurjchem-1251	155	41	4.59	4.59	NUM
eurjchem-1251	155	42	)	)	PUNCT
eurjchem-1251	155	43	,	,	PUNCT
eurjchem-1251	155	44	288	288	NUM
eurjchem-1251	155	45	(	(	PUNCT
eurjchem-1251	155	46	3.35	3.35	NUM
eurjchem-1251	155	47	)	)	PUNCT
eurjchem-1251	155	48	,	,	PUNCT
eurjchem-1251	155	49	213	213	NUM
eurjchem-1251	155	50	(	(	PUNCT
eurjchem-1251	155	51	3.30	3.30	NUM
eurjchem-1251	155	52	)	)	PUNCT
eurjchem-1251	155	53	,	,	PUNCT
eurjchem-1251	155	54	178	178	NUM
eurjchem-1251	155	55	(	(	PUNCT
eurjchem-1251	155	56	25.40	25.40	NUM
eurjchem-1251	155	57	)	)	PUNCT
eurjchem-1251	155	58	,	,	PUNCT
eurjchem-1251	155	59	103	103	NUM
eurjchem-1251	155	60	(	(	PUNCT
eurjchem-1251	155	61	4.85	4.85	NUM
eurjchem-1251	155	62	)	)	PUNCT
eurjchem-1251	155	63	,	,	PUNCT
eurjchem-1251	155	64	69	69	NUM
eurjchem-1251	155	65	(	(	PUNCT
eurjchem-1251	155	66	100	100	NUM
eurjchem-1251	155	67	)	)	PUNCT
eurjchem-1251	155	68	.	.	PUNCT
eurjchem-1251	156	1	anal	anal	PROPN
eurjchem-1251	156	2	.	.	PUNCT
eurjchem-1251	156	3	calcd	calcd	NOUN
eurjchem-1251	156	4	.	.	PUNCT
eurjchem-1251	157	1	for	for	ADP
eurjchem-1251	157	2	c25h17n3o2	c25h17n3o2	PROPN
eurjchem-1251	157	3	:	:	PUNCT
eurjchem-1251	157	4	c	c	X
eurjchem-1251	157	5	,	,	PUNCT
eurjchem-1251	157	6	76.71	76.71	NUM
eurjchem-1251	157	7	;	;	PUNCT
eurjchem-1251	157	8	h	h	NOUN
eurjchem-1251	157	9	,	,	PUNCT
eurjchem-1251	157	10	4.38	4.38	NUM
eurjchem-1251	157	11	;	;	PUNCT
eurjchem-1251	157	12	n	n	CCONJ
eurjchem-1251	157	13	,	,	PUNCT
eurjchem-1251	157	14	10.74	10.74	NUM
eurjchem-1251	157	15	.	.	PUNCT
eurjchem-1251	157	16	found	find	VERB
eurjchem-1251	157	17	:	:	PUNCT
eurjchem-1251	158	1	c	c	X
eurjchem-1251	158	2	,	,	PUNCT
eurjchem-1251	158	3	76.50	76.50	NUM
eurjchem-1251	158	4	;	;	PUNCT
eurjchem-1251	158	5	h	h	NOUN
eurjchem-1251	158	6	,	,	PUNCT
eurjchem-1251	158	7	4.20	4.20	NUM
eurjchem-1251	158	8	;	;	PUNCT
eurjchem-1251	158	9	n	n	CCONJ
eurjchem-1251	158	10	,	,	PUNCT
eurjchem-1251	158	11	10.60	10.60	NUM
eurjchem-1251	158	12	%	%	NOUN
eurjchem-1251	158	13	.	.	PUNCT
eurjchem-1251	159	1	2.2.13	2.2.13	NUM
eurjchem-1251	159	2	.	.	PUNCT
eurjchem-1251	160	1	synthesis	synthesis	NOUN
eurjchem-1251	160	2	of	of	ADP
eurjchem-1251	160	3	ethyl	ethyl	PROPN
eurjchem-1251	160	4	oxo[(4,5,6‐triphenylpyridazin‐3‐	oxo[(4,5,6‐triphenylpyridazin‐3‐	PRON
eurjchem-1251	160	5	yl)amino]acetate	yl)amino]acetate	NOUN
eurjchem-1251	160	6	(	(	PUNCT
eurjchem-1251	160	7	10a	10a	NOUN
eurjchem-1251	160	8	)	)	PUNCT
eurjchem-1251	160	9	a	a	DET
eurjchem-1251	160	10	mixture	mixture	NOUN
eurjchem-1251	160	11	of	of	ADP
eurjchem-1251	160	12	compound	compound	NOUN
eurjchem-1251	160	13	5	5	NUM
eurjchem-1251	160	14	(	(	PUNCT
eurjchem-1251	160	15	0.5	0.5	NUM
eurjchem-1251	160	16	g	g	NOUN
eurjchem-1251	160	17	,	,	PUNCT
eurjchem-1251	160	18	1.55	1.55	NUM
eurjchem-1251	160	19	mmol	mmol	NOUN
eurjchem-1251	160	20	)	)	PUNCT
eurjchem-1251	160	21	and	and	CCONJ
eurjchem-1251	160	22	diethyl	diethyl	PROPN
eurjchem-1251	160	23	oxalate	oxalate	NOUN
eurjchem-1251	160	24	(	(	PUNCT
eurjchem-1251	160	25	0.16	0.16	NUM
eurjchem-1251	160	26	ml	ml	NOUN
eurjchem-1251	160	27	,	,	PUNCT
eurjchem-1251	160	28	1.55	1.55	NUM
eurjchem-1251	160	29	mmol	mmol	NOUN
eurjchem-1251	160	30	)	)	PUNCT
eurjchem-1251	160	31	was	be	AUX
eurjchem-1251	160	32	heated	heat	VERB
eurjchem-1251	160	33	under	under	ADP
eurjchem-1251	160	34	reflux	reflux	NOUN
eurjchem-1251	160	35	for	for	ADP
eurjchem-1251	160	36	3	3	NUM
eurjchem-1251	160	37	h.	h.	NOUN
eurjchem-1251	160	38	after	after	ADP
eurjchem-1251	160	39	cooling	cool	VERB
eurjchem-1251	160	40	,	,	PUNCT
eurjchem-1251	160	41	the	the	DET
eurjchem-1251	160	42	reaction	reaction	NOUN
eurjchem-1251	160	43	mixture	mixture	NOUN
eurjchem-1251	160	44	was	be	AUX
eurjchem-1251	160	45	treated	treat	VERB
eurjchem-1251	160	46	with	with	ADP
eurjchem-1251	160	47	diethyl	diethyl	NOUN
eurjchem-1251	160	48	ether	ether	NOUN
eurjchem-1251	160	49	(	(	PUNCT
eurjchem-1251	160	50	50	50	NUM
eurjchem-1251	160	51	ml	ml	NOUN
eurjchem-1251	160	52	)	)	PUNCT
eurjchem-1251	160	53	,	,	PUNCT
eurjchem-1251	160	54	and	and	CCONJ
eurjchem-1251	160	55	the	the	DET
eurjchem-1251	160	56	solid	solid	ADJ
eurjchem-1251	160	57	product	product	NOUN
eurjchem-1251	160	58	formed	form	VERB
eurjchem-1251	160	59	was	be	AUX
eurjchem-1251	160	60	filtered	filter	VERB
eurjchem-1251	160	61	off	off	ADP
eurjchem-1251	160	62	,	,	PUNCT
eurjchem-1251	160	63	dried	dry	VERB
eurjchem-1251	160	64	,	,	PUNCT
eurjchem-1251	160	65	and	and	CCONJ
eurjchem-1251	160	66	recrystallized	recrystallize	VERB
eurjchem-1251	160	67	from	from	ADP
eurjchem-1251	160	68	ethanol	ethanol	NOUN
eurjchem-1251	160	69	(	(	PUNCT
eurjchem-1251	160	70	scheme	scheme	NOUN
eurjchem-1251	160	71	3	3	NUM
eurjchem-1251	160	72	)	)	PUNCT
eurjchem-1251	160	73	.	.	PUNCT
eurjchem-1251	161	1	color	color	NOUN
eurjchem-1251	161	2	:	:	PUNCT
eurjchem-1251	161	3	yellow	yellow	ADJ
eurjchem-1251	161	4	.	.	PUNCT
eurjchem-1251	162	1	yield	yield	NOUN
eurjchem-1251	162	2	:	:	PUNCT
eurjchem-1251	162	3	80.92	80.92	NUM
eurjchem-1251	162	4	%	%	NOUN
eurjchem-1251	162	5	.	.	PUNCT
eurjchem-1251	163	1	m.p	m.p	PROPN
eurjchem-1251	163	2	.	.	PROPN
eurjchem-1251	163	3	:	:	PUNCT
eurjchem-1251	164	1	217‐219	217‐219	NUM
eurjchem-1251	164	2	°	°	SYM
eurjchem-1251	164	3	c	c	NOUN
eurjchem-1251	164	4	.	.	PUNCT
eurjchem-1251	165	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	165	2	(	(	PUNCT
eurjchem-1251	165	3	kbr	kbr	PROPN
eurjchem-1251	165	4	,	,	PUNCT
eurjchem-1251	165	5	ν	ν	PROPN
eurjchem-1251	165	6	,	,	PUNCT
eurjchem-1251	165	7	cm‐1	cm‐1	PROPN
eurjchem-1251	165	8	):	):	PUNCT
eurjchem-1251	165	9	3425	3425	NUM
eurjchem-1251	165	10	(	(	PUNCT
eurjchem-1251	165	11	nh	nh	NOUN
eurjchem-1251	165	12	amide	amide	PROPN
eurjchem-1251	165	13	)	)	PUNCT
eurjchem-1251	165	14	,	,	PUNCT
eurjchem-1251	165	15	3059	3059	NUM
eurjchem-1251	165	16	(	(	PUNCT
eurjchem-1251	165	17	ch	ch	NOUN
eurjchem-1251	165	18	arom	arom	NOUN
eurjchem-1251	165	19	.	.	PUNCT
eurjchem-1251	165	20	)	)	PUNCT
eurjchem-1251	165	21	,	,	PUNCT
eurjchem-1251	165	22	2976	2976	NUM
eurjchem-1251	165	23	,	,	PUNCT
eurjchem-1251	165	24	2933	2933	NUM
eurjchem-1251	165	25	(	(	PUNCT
eurjchem-1251	165	26	ch	ch	NOUN
eurjchem-1251	165	27	aliph	aliph	PROPN
eurjchem-1251	165	28	.	.	PUNCT
eurjchem-1251	165	29	)	)	PUNCT
eurjchem-1251	165	30	,	,	PUNCT
eurjchem-1251	165	31	1729	1729	NUM
eurjchem-1251	165	32	(	(	PUNCT
eurjchem-1251	165	33	c	c	NOUN
eurjchem-1251	165	34	=	=	NOUN
eurjchem-1251	165	35	o	o	NOUN
eurjchem-1251	165	36	ester	ester	NOUN
eurjchem-1251	165	37	)	)	PUNCT
eurjchem-1251	165	38	,	,	PUNCT
eurjchem-1251	165	39	1682	1682	NUM
eurjchem-1251	165	40	(	(	PUNCT
eurjchem-1251	165	41	c	c	NOUN
eurjchem-1251	165	42	=	=	NOUN
eurjchem-1251	165	43	o	o	NOUN
eurjchem-1251	165	44	amide	amide	NOUN
eurjchem-1251	165	45	)	)	PUNCT
eurjchem-1251	165	46	,	,	PUNCT
eurjchem-1251	165	47	1226	1226	NUM
eurjchem-1251	165	48	(	(	PUNCT
eurjchem-1251	165	49	c‐o	c‐o	NOUN
eurjchem-1251	165	50	)	)	PUNCT
eurjchem-1251	165	51	.	.	PUNCT
eurjchem-1251	166	1	1h	1h	NUM
eurjchem-1251	166	2	nmr	nmr	NOUN
eurjchem-1251	166	3	(	(	PUNCT
eurjchem-1251	166	4	300	300	NUM
eurjchem-1251	166	5	mhz	mhz	NOUN
eurjchem-1251	166	6	,	,	PUNCT
eurjchem-1251	166	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	166	8	,	,	PUNCT
eurjchem-1251	166	9	δ	δ	PROPN
eurjchem-1251	166	10	,	,	PUNCT
eurjchem-1251	166	11	ppm	ppm	NUM
eurjchem-1251	166	12	):	):	PUNCT
eurjchem-1251	166	13	1.26	1.26	NUM
eurjchem-1251	166	14	(	(	PUNCT
eurjchem-1251	166	15	t	t	PROPN
eurjchem-1251	166	16	,	,	PUNCT
eurjchem-1251	166	17	j	j	PROPN
eurjchem-1251	166	18	=	=	SYM
eurjchem-1251	166	19	7.5	7.5	NUM
eurjchem-1251	166	20	hz	hz	NOUN
eurjchem-1251	166	21	,	,	PUNCT
eurjchem-1251	166	22	3h	3h	NUM
eurjchem-1251	166	23	,	,	PUNCT
eurjchem-1251	166	24	ch3	ch3	PROPN
eurjchem-1251	166	25	)	)	PUNCT
eurjchem-1251	166	26	,	,	PUNCT
eurjchem-1251	166	27	3.91	3.91	NUM
eurjchem-1251	166	28	(	(	PUNCT
eurjchem-1251	166	29	q	q	NOUN
eurjchem-1251	166	30	,	,	PUNCT
eurjchem-1251	166	31	2h	2h	NUM
eurjchem-1251	166	32	,	,	PUNCT
eurjchem-1251	166	33	ch2	ch2	PROPN
eurjchem-1251	166	34	)	)	PUNCT
eurjchem-1251	166	35	,	,	PUNCT
eurjchem-1251	166	36	6.99‐7.62	6.99‐7.62	NUM
eurjchem-1251	166	37	(	(	PUNCT
eurjchem-1251	166	38	m	m	PROPN
eurjchem-1251	166	39	,	,	PUNCT
eurjchem-1251	166	40	15h	15h	NUM
eurjchem-1251	166	41	,	,	PUNCT
eurjchem-1251	166	42	3ph	3ph	NOUN
eurjchem-1251	166	43	)	)	PUNCT
eurjchem-1251	166	44	,	,	PUNCT
eurjchem-1251	166	45	7.86	7.86	NUM
eurjchem-1251	166	46	(	(	PUNCT
eurjchem-1251	166	47	s	s	PROPN
eurjchem-1251	166	48	,	,	PUNCT
eurjchem-1251	166	49	1h	1h	NUM
eurjchem-1251	166	50	,	,	PUNCT
eurjchem-1251	166	51	nh	nh	PROPN
eurjchem-1251	166	52	)	)	PUNCT
eurjchem-1251	166	53	.	.	PUNCT
eurjchem-1251	167	1	ms	ms	NOUN
eurjchem-1251	167	2	(	(	PUNCT
eurjchem-1251	167	3	ei	ei	PROPN
eurjchem-1251	167	4	,	,	PUNCT
eurjchem-1251	167	5	m	m	PROPN
eurjchem-1251	167	6	/	/	SYM
eurjchem-1251	167	7	z	z	PROPN
eurjchem-1251	167	8	(	(	PUNCT
eurjchem-1251	167	9	%	%	NOUN
eurjchem-1251	167	10	)	)	PUNCT
eurjchem-1251	167	11	):	):	PUNCT
eurjchem-1251	167	12	423	423	NUM
eurjchem-1251	167	13	(	(	PUNCT
eurjchem-1251	167	14	m+	m+	NUM
eurjchem-1251	167	15	,	,	PUNCT
eurjchem-1251	167	16	6.77	6.77	NUM
eurjchem-1251	167	17	)	)	PUNCT
eurjchem-1251	167	18	,	,	PUNCT
eurjchem-1251	167	19	422	422	NUM
eurjchem-1251	167	20	(	(	PUNCT
eurjchem-1251	167	21	[	[	X
eurjchem-1251	167	22	m‐1]+	m‐1]+	ADJ
eurjchem-1251	167	23	,	,	PUNCT
eurjchem-1251	167	24	10.68	10.68	NUM
eurjchem-1251	167	25	)	)	PUNCT
eurjchem-1251	167	26	,	,	PUNCT
eurjchem-1251	167	27	378	378	NUM
eurjchem-1251	167	28	(	(	PUNCT
eurjchem-1251	167	29	14.28	14.28	NUM
eurjchem-1251	167	30	)	)	PUNCT
eurjchem-1251	167	31	,	,	PUNCT
eurjchem-1251	167	32	350	350	NUM
eurjchem-1251	167	33	(	(	PUNCT
eurjchem-1251	167	34	100	100	NUM
eurjchem-1251	167	35	)	)	PUNCT
eurjchem-1251	167	36	,	,	PUNCT
eurjchem-1251	167	37	322	322	NUM
eurjchem-1251	167	38	(	(	PUNCT
eurjchem-1251	167	39	3.48	3.48	NUM
eurjchem-1251	167	40	)	)	PUNCT
eurjchem-1251	167	41	,	,	PUNCT
eurjchem-1251	167	42	307	307	NUM
eurjchem-1251	167	43	(	(	PUNCT
eurjchem-1251	167	44	5.11	5.11	NUM
eurjchem-1251	167	45	)	)	PUNCT
eurjchem-1251	167	46	,	,	PUNCT
eurjchem-1251	167	47	206	206	NUM
eurjchem-1251	167	48	(	(	PUNCT
eurjchem-1251	167	49	0.64	0.64	NUM
eurjchem-1251	167	50	)	)	PUNCT
eurjchem-1251	167	51	,	,	PUNCT
eurjchem-1251	167	52	178	178	NUM
eurjchem-1251	167	53	(	(	PUNCT
eurjchem-1251	167	54	9.14	9.14	NUM
eurjchem-1251	167	55	)	)	PUNCT
eurjchem-1251	167	56	,	,	PUNCT
eurjchem-1251	167	57	77	77	NUM
eurjchem-1251	167	58	(	(	PUNCT
eurjchem-1251	167	59	10.57	10.57	NUM
eurjchem-1251	167	60	)	)	PUNCT
eurjchem-1251	167	61	,	,	PUNCT
eurjchem-1251	167	62	76	76	NUM
eurjchem-1251	167	63	(	(	PUNCT
eurjchem-1251	167	64	2.03	2.03	NUM
eurjchem-1251	167	65	)	)	PUNCT
eurjchem-1251	167	66	.	.	PUNCT
eurjchem-1251	168	1	anal	anal	PROPN
eurjchem-1251	168	2	.	.	PUNCT
eurjchem-1251	168	3	calcd	calcd	NOUN
eurjchem-1251	168	4	.	.	PUNCT
eurjchem-1251	169	1	for	for	ADP
eurjchem-1251	169	2	c26h21n3o3	c26h21n3o3	NOUN
eurjchem-1251	169	3	:	:	PUNCT
eurjchem-1251	169	4	c	c	X
eurjchem-1251	169	5	,	,	PUNCT
eurjchem-1251	169	6	73.74	73.74	NUM
eurjchem-1251	169	7	;	;	PUNCT
eurjchem-1251	169	8	h	h	NOUN
eurjchem-1251	169	9	,	,	PUNCT
eurjchem-1251	169	10	5.00	5.00	NUM
eurjchem-1251	169	11	;	;	PUNCT
eurjchem-1251	169	12	n	n	CCONJ
eurjchem-1251	169	13	,	,	PUNCT
eurjchem-1251	169	14	9.92	9.92	NUM
eurjchem-1251	169	15	.	.	PUNCT
eurjchem-1251	169	16	found	find	VERB
eurjchem-1251	169	17	:	:	PUNCT
eurjchem-1251	169	18	c	c	NOUN
eurjchem-1251	169	19	74.10	74.10	NUM
eurjchem-1251	169	20	;	;	PUNCT
eurjchem-1251	169	21	h	h	NOUN
eurjchem-1251	169	22	,	,	PUNCT
eurjchem-1251	169	23	5.40	5.40	NUM
eurjchem-1251	169	24	;	;	PUNCT
eurjchem-1251	169	25	n	n	CCONJ
eurjchem-1251	169	26	,	,	PUNCT
eurjchem-1251	169	27	10.10	10.10	NUM
eurjchem-1251	169	28	%	%	NOUN
eurjchem-1251	169	29	.	.	PUNCT
eurjchem-1251	170	1	2.2.14	2.2.14	X
eurjchem-1251	170	2	.	.	PUNCT
eurjchem-1251	171	1	synthesis	synthesis	NOUN
eurjchem-1251	171	2	of	of	ADP
eurjchem-1251	171	3	2‐cyano‐n‐(4,5,6‐triphenylpyridazin‐3‐	2‐cyano‐n‐(4,5,6‐triphenylpyridazin‐3‐	NUM
eurjchem-1251	171	4	yl)acetamide	yl)acetamide	NOUN
eurjchem-1251	171	5	(	(	PUNCT
eurjchem-1251	171	6	10b	10b	NOUN
eurjchem-1251	171	7	)	)	PUNCT
eurjchem-1251	171	8	a	a	DET
eurjchem-1251	171	9	mixture	mixture	NOUN
eurjchem-1251	171	10	of	of	ADP
eurjchem-1251	171	11	compound	compound	NOUN
eurjchem-1251	171	12	5	5	NUM
eurjchem-1251	171	13	(	(	PUNCT
eurjchem-1251	171	14	0.5	0.5	NUM
eurjchem-1251	171	15	g	g	NOUN
eurjchem-1251	171	16	,	,	PUNCT
eurjchem-1251	171	17	1.55	1.55	NUM
eurjchem-1251	171	18	mmol	mmol	NOUN
eurjchem-1251	171	19	)	)	PUNCT
eurjchem-1251	171	20	and	and	CCONJ
eurjchem-1251	171	21	ethyl	ethyl	PROPN
eurjchem-1251	171	22	cyanoacetate	cyanoacetate	NOUN
eurjchem-1251	171	23	(	(	PUNCT
eurjchem-1251	171	24	0.16	0.16	NUM
eurjchem-1251	171	25	ml	ml	NOUN
eurjchem-1251	171	26	,	,	PUNCT
eurjchem-1251	171	27	1.55	1.55	NUM
eurjchem-1251	171	28	mmol	mmol	NOUN
eurjchem-1251	171	29	)	)	PUNCT
eurjchem-1251	171	30	was	be	AUX
eurjchem-1251	171	31	heated	heat	VERB
eurjchem-1251	171	32	under	under	ADP
eurjchem-1251	171	33	reflux	reflux	NOUN
eurjchem-1251	171	34	for	for	ADP
eurjchem-1251	171	35	1	1	NUM
eurjchem-1251	171	36	h.	h.	NOUN
eurjchem-1251	171	37	the	the	DET
eurjchem-1251	171	38	cooled	cool	VERB
eurjchem-1251	171	39	reaction	reaction	NOUN
eurjchem-1251	171	40	mixture	mixture	NOUN
eurjchem-1251	171	41	was	be	AUX
eurjchem-1251	171	42	treated	treat	VERB
eurjchem-1251	171	43	with	with	ADP
eurjchem-1251	171	44	diethyl	diethyl	NOUN
eurjchem-1251	171	45	ether	ether	NOUN
eurjchem-1251	171	46	(	(	PUNCT
eurjchem-1251	171	47	50	50	NUM
eurjchem-1251	171	48	ml	ml	NOUN
eurjchem-1251	171	49	)	)	PUNCT
eurjchem-1251	171	50	.	.	PUNCT
eurjchem-1251	172	1	the	the	DET
eurjchem-1251	172	2	solid	solid	ADJ
eurjchem-1251	172	3	product	product	NOUN
eurjchem-1251	172	4	was	be	AUX
eurjchem-1251	172	5	filtered	filter	VERB
eurjchem-1251	172	6	off	off	ADP
eurjchem-1251	172	7	,	,	PUNCT
eurjchem-1251	172	8	dried	dry	VERB
eurjchem-1251	172	9	and	and	CCONJ
eurjchem-1251	172	10	recrystallized	recrystallize	VERB
eurjchem-1251	172	11	from	from	ADP
eurjchem-1251	172	12	ethanol	ethanol	NOUN
eurjchem-1251	172	13	(	(	PUNCT
eurjchem-1251	172	14	scheme	scheme	NOUN
eurjchem-1251	172	15	3	3	NUM
eurjchem-1251	172	16	)	)	PUNCT
eurjchem-1251	172	17	.	.	PUNCT
eurjchem-1251	173	1	color	color	NOUN
eurjchem-1251	173	2	:	:	PUNCT
eurjchem-1251	173	3	brown	brown	ADJ
eurjchem-1251	173	4	.	.	PUNCT
eurjchem-1251	174	1	yield	yield	NOUN
eurjchem-1251	174	2	:	:	PUNCT
eurjchem-1251	174	3	79.51	79.51	NUM
eurjchem-1251	174	4	%	%	NOUN
eurjchem-1251	174	5	.	.	PUNCT
eurjchem-1251	175	1	m.p	m.p	PROPN
eurjchem-1251	175	2	.	.	PROPN
eurjchem-1251	175	3	:	:	PUNCT
eurjchem-1251	176	1	178‐180	178‐180	NUM
eurjchem-1251	176	2	°	°	SYM
eurjchem-1251	176	3	c	c	X
eurjchem-1251	176	4	.	.	PUNCT
eurjchem-1251	177	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	177	2	(	(	PUNCT
eurjchem-1251	177	3	kbr	kbr	PROPN
eurjchem-1251	177	4	,	,	PUNCT
eurjchem-1251	177	5	ν	ν	PROPN
eurjchem-1251	177	6	,	,	PUNCT
eurjchem-1251	177	7	cm‐1	cm‐1	PROPN
eurjchem-1251	177	8	):	):	PUNCT
eurjchem-1251	177	9	3184	3184	NUM
eurjchem-1251	177	10	(	(	PUNCT
eurjchem-1251	177	11	nh	nh	NOUN
eurjchem-1251	177	12	amide	amide	PROPN
eurjchem-1251	177	13	)	)	PUNCT
eurjchem-1251	177	14	,	,	PUNCT
eurjchem-1251	177	15	3060	3060	NUM
eurjchem-1251	177	16	(	(	PUNCT
eurjchem-1251	177	17	ch	ch	NOUN
eurjchem-1251	177	18	arom	arom	NOUN
eurjchem-1251	177	19	.	.	PUNCT
eurjchem-1251	177	20	)	)	PUNCT
eurjchem-1251	177	21	,	,	PUNCT
eurjchem-1251	177	22	2985	2985	NUM
eurjchem-1251	177	23	(	(	PUNCT
eurjchem-1251	177	24	ch	ch	NOUN
eurjchem-1251	177	25	aliph	aliph	PROPN
eurjchem-1251	177	26	.	.	PUNCT
eurjchem-1251	177	27	)	)	PUNCT
eurjchem-1251	177	28	,	,	PUNCT
eurjchem-1251	177	29	2204	2204	NUM
eurjchem-1251	177	30	(	(	PUNCT
eurjchem-1251	177	31	c≡n	c≡n	PROPN
eurjchem-1251	177	32	)	)	PUNCT
eurjchem-1251	177	33	,	,	PUNCT
eurjchem-1251	177	34	1658	1658	NUM
eurjchem-1251	177	35	(	(	PUNCT
eurjchem-1251	177	36	c	c	NOUN
eurjchem-1251	177	37	=	=	NOUN
eurjchem-1251	177	38	o	o	NOUN
eurjchem-1251	177	39	amide	amide	NOUN
eurjchem-1251	177	40	)	)	PUNCT
eurjchem-1251	177	41	.	.	PUNCT
eurjchem-1251	178	1	1h	1h	NUM
eurjchem-1251	178	2	nmr	nmr	NOUN
eurjchem-1251	178	3	(	(	PUNCT
eurjchem-1251	178	4	300	300	NUM
eurjchem-1251	178	5	mhz	mhz	NOUN
eurjchem-1251	178	6	,	,	PUNCT
eurjchem-1251	178	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	178	8	,	,	PUNCT
eurjchem-1251	178	9	δ	δ	PROPN
eurjchem-1251	178	10	,	,	PUNCT
eurjchem-1251	178	11	ppm	ppm	NUM
eurjchem-1251	178	12	):	):	PUNCT
eurjchem-1251	178	13	3.58	3.58	NUM
eurjchem-1251	178	14	(	(	PUNCT
eurjchem-1251	178	15	s	s	PROPN
eurjchem-1251	178	16	,	,	PUNCT
eurjchem-1251	178	17	2h	2h	NUM
eurjchem-1251	178	18	,	,	PUNCT
eurjchem-1251	178	19	ch2	ch2	PROPN
eurjchem-1251	178	20	)	)	PUNCT
eurjchem-1251	178	21	,	,	PUNCT
eurjchem-1251	178	22	6.51	6.51	NUM
eurjchem-1251	178	23	(	(	PUNCT
eurjchem-1251	178	24	s	s	PROPN
eurjchem-1251	178	25	,	,	PUNCT
eurjchem-1251	178	26	1h	1h	NUM
eurjchem-1251	178	27	,	,	PUNCT
eurjchem-1251	178	28	nh	nh	PROPN
eurjchem-1251	178	29	)	)	PUNCT
eurjchem-1251	178	30	,	,	PUNCT
eurjchem-1251	178	31	6.97‐7.42	6.97‐7.42	NUM
eurjchem-1251	178	32	(	(	PUNCT
eurjchem-1251	178	33	m	m	PROPN
eurjchem-1251	178	34	,	,	PUNCT
eurjchem-1251	178	35	15h	15h	NUM
eurjchem-1251	178	36	,	,	PUNCT
eurjchem-1251	178	37	3ph	3ph	NOUN
eurjchem-1251	178	38	)	)	PUNCT
eurjchem-1251	178	39	.	.	PUNCT
eurjchem-1251	179	1	ms	ms	NOUN
eurjchem-1251	179	2	(	(	PUNCT
eurjchem-1251	179	3	ei	ei	PROPN
eurjchem-1251	179	4	,	,	PUNCT
eurjchem-1251	179	5	m	m	PROPN
eurjchem-1251	179	6	/	/	SYM
eurjchem-1251	179	7	z	z	PROPN
eurjchem-1251	179	8	(	(	PUNCT
eurjchem-1251	179	9	%	%	NOUN
eurjchem-1251	179	10	)	)	PUNCT
eurjchem-1251	179	11	):	):	PUNCT
eurjchem-1251	179	12	390	390	NUM
eurjchem-1251	179	13	(	(	PUNCT
eurjchem-1251	179	14	m+	m+	NUM
eurjchem-1251	179	15	,	,	PUNCT
eurjchem-1251	179	16	79.96	79.96	NUM
eurjchem-1251	179	17	)	)	PUNCT
eurjchem-1251	179	18	,	,	PUNCT
eurjchem-1251	179	19	373	373	NUM
eurjchem-1251	179	20	(	(	PUNCT
eurjchem-1251	179	21	12.58	12.58	NUM
eurjchem-1251	179	22	)	)	PUNCT
eurjchem-1251	179	23	,	,	PUNCT
eurjchem-1251	179	24	364	364	NUM
eurjchem-1251	179	25	(	(	PUNCT
eurjchem-1251	179	26	5.13	5.13	NUM
eurjchem-1251	179	27	)	)	PUNCT
eurjchem-1251	179	28	,	,	PUNCT
eurjchem-1251	179	29	362	362	NUM
eurjchem-1251	179	30	(	(	PUNCT
eurjchem-1251	179	31	11.96	11.96	NUM
eurjchem-1251	179	32	)	)	PUNCT
eurjchem-1251	179	33	,	,	PUNCT
eurjchem-1251	179	34	322	322	NUM
eurjchem-1251	179	35	(	(	PUNCT
eurjchem-1251	179	36	100	100	NUM
eurjchem-1251	179	37	)	)	PUNCT
eurjchem-1251	179	38	,	,	PUNCT
eurjchem-1251	179	39	313	313	NUM
eurjchem-1251	179	40	(	(	PUNCT
eurjchem-1251	179	41	12.83	12.83	NUM
eurjchem-1251	179	42	)	)	PUNCT
eurjchem-1251	179	43	,	,	PUNCT
eurjchem-1251	179	44	307	307	NUM
eurjchem-1251	179	45	(	(	PUNCT
eurjchem-1251	179	46	20.20	20.20	NUM
eurjchem-1251	179	47	)	)	PUNCT
eurjchem-1251	179	48	,	,	PUNCT
eurjchem-1251	179	49	287	287	NUM
eurjchem-1251	179	50	(	(	PUNCT
eurjchem-1251	179	51	25.24	25.24	NUM
eurjchem-1251	179	52	)	)	PUNCT
eurjchem-1251	179	53	,	,	PUNCT
eurjchem-1251	179	54	178	178	NUM
eurjchem-1251	179	55	(	(	PUNCT
eurjchem-1251	179	56	30.92	30.92	NUM
eurjchem-1251	179	57	)	)	PUNCT
eurjchem-1251	179	58	,	,	PUNCT
eurjchem-1251	179	59	77	77	NUM
eurjchem-1251	179	60	(	(	PUNCT
eurjchem-1251	179	61	42.05	42.05	NUM
eurjchem-1251	179	62	)	)	PUNCT
eurjchem-1251	179	63	,	,	PUNCT
eurjchem-1251	179	64	68	68	NUM
eurjchem-1251	179	65	(	(	PUNCT
eurjchem-1251	179	66	71.96	71.96	NUM
eurjchem-1251	179	67	)	)	PUNCT
eurjchem-1251	179	68	.	.	PUNCT
eurjchem-1251	180	1	anal	anal	PROPN
eurjchem-1251	180	2	.	.	PUNCT
eurjchem-1251	180	3	calcd	calcd	NOUN
eurjchem-1251	180	4	.	.	PUNCT
eurjchem-1251	181	1	for	for	ADP
eurjchem-1251	181	2	c25h18n4o	c25h18n4o	NOUN
eurjchem-1251	181	3	:	:	PUNCT
eurjchem-1251	181	4	c	c	X
eurjchem-1251	181	5	,	,	PUNCT
eurjchem-1251	181	6	76.91	76.91	NUM
eurjchem-1251	181	7	;	;	PUNCT
eurjchem-1251	181	8	h	h	NOUN
eurjchem-1251	181	9	,	,	PUNCT
eurjchem-1251	181	10	4.65	4.65	NUM
eurjchem-1251	181	11	;	;	PUNCT
eurjchem-1251	181	12	n	n	CCONJ
eurjchem-1251	181	13	,	,	PUNCT
eurjchem-1251	181	14	14.35	14.35	NUM
eurjchem-1251	181	15	.	.	PUNCT
eurjchem-1251	181	16	found	find	VERB
eurjchem-1251	181	17	:	:	PUNCT
eurjchem-1251	182	1	c	c	X
eurjchem-1251	182	2	:	:	PUNCT
eurjchem-1251	182	3	77.30	77.30	NUM
eurjchem-1251	182	4	;	;	PUNCT
eurjchem-1251	182	5	h	h	NOUN
eurjchem-1251	182	6	,	,	PUNCT
eurjchem-1251	182	7	4.90	4.90	NUM
eurjchem-1251	182	8	;	;	PUNCT
eurjchem-1251	182	9	n	n	CCONJ
eurjchem-1251	182	10	,	,	PUNCT
eurjchem-1251	182	11	14.70	14.70	NUM
eurjchem-1251	182	12	%	%	NOUN
eurjchem-1251	182	13	.	.	PUNCT
eurjchem-1251	183	1	2.2.15	2.2.15	X
eurjchem-1251	183	2	.	.	PUNCT
eurjchem-1251	183	3	synthesis	synthesis	NOUN
eurjchem-1251	183	4	of	of	ADP
eurjchem-1251	183	5	4‐amino‐7,8,9‐triphenyl‐2h‐pyrimido	4‐amino‐7,8,9‐triphenyl‐2h‐pyrimido	NOUN
eurjchem-1251	183	6	[	[	X
eurjchem-1251	183	7	1,2‐b]pyridazin‐2‐one	1,2‐b]pyridazin‐2‐one	NOUN
eurjchem-1251	183	8	(	(	PUNCT
eurjchem-1251	183	9	11a	11a	NOUN
eurjchem-1251	183	10	)	)	PUNCT
eurjchem-1251	183	11	a	a	DET
eurjchem-1251	183	12	mixture	mixture	NOUN
eurjchem-1251	183	13	of	of	ADP
eurjchem-1251	183	14	compound	compound	NOUN
eurjchem-1251	183	15	5	5	NUM
eurjchem-1251	183	16	(	(	PUNCT
eurjchem-1251	183	17	0.5	0.5	NUM
eurjchem-1251	183	18	g	g	NOUN
eurjchem-1251	183	19	,	,	PUNCT
eurjchem-1251	183	20	1.55	1.55	NUM
eurjchem-1251	183	21	mmol	mmol	NOUN
eurjchem-1251	183	22	)	)	PUNCT
eurjchem-1251	183	23	,	,	PUNCT
eurjchem-1251	183	24	ethyl	ethyl	PROPN
eurjchem-1251	183	25	cyanoacetate	cyanoacetate	NOUN
eurjchem-1251	183	26	(	(	PUNCT
eurjchem-1251	183	27	0.16	0.16	NUM
eurjchem-1251	183	28	ml	ml	NOUN
eurjchem-1251	183	29	,	,	PUNCT
eurjchem-1251	183	30	1.55	1.55	NUM
eurjchem-1251	183	31	mmol	mmol	NOUN
eurjchem-1251	183	32	)	)	PUNCT
eurjchem-1251	183	33	,	,	PUNCT
eurjchem-1251	183	34	and	and	CCONJ
eurjchem-1251	183	35	excess	excess	ADJ
eurjchem-1251	183	36	polyphosp‐	polyphosp‐	X
eurjchem-1251	183	37	horic	horic	ADJ
eurjchem-1251	183	38	acid	acid	NOUN
eurjchem-1251	183	39	(	(	PUNCT
eurjchem-1251	183	40	1	1	NUM
eurjchem-1251	183	41	g	g	NOUN
eurjchem-1251	183	42	)	)	PUNCT
eurjchem-1251	183	43	was	be	AUX
eurjchem-1251	183	44	heated	heat	VERB
eurjchem-1251	183	45	at	at	ADP
eurjchem-1251	183	46	110	110	NUM
eurjchem-1251	183	47	°	°	NOUN
eurjchem-1251	183	48	c	c	NOUN
eurjchem-1251	183	49	for	for	ADP
eurjchem-1251	183	50	6	6	NUM
eurjchem-1251	183	51	h	h	NOUN
eurjchem-1251	183	52	with	with	ADP
eurjchem-1251	183	53	stirring	stirring	NOUN
eurjchem-1251	183	54	.	.	PUNCT
eurjchem-1251	184	1	the	the	DET
eurjchem-1251	184	2	cooled	cool	VERB
eurjchem-1251	184	3	mixture	mixture	NOUN
eurjchem-1251	184	4	was	be	AUX
eurjchem-1251	184	5	poured	pour	VERB
eurjchem-1251	184	6	into	into	ADP
eurjchem-1251	184	7	ice	ice	NOUN
eurjchem-1251	184	8	water	water	NOUN
eurjchem-1251	184	9	(	(	PUNCT
eurjchem-1251	184	10	200	200	NUM
eurjchem-1251	184	11	ml	ml	NOUN
eurjchem-1251	184	12	)	)	PUNCT
eurjchem-1251	184	13	,	,	PUNCT
eurjchem-1251	184	14	and	and	CCONJ
eurjchem-1251	184	15	the	the	DET
eurjchem-1251	184	16	solution	solution	NOUN
eurjchem-1251	184	17	was	be	AUX
eurjchem-1251	184	18	neutralised	neutralise	VERB
eurjchem-1251	184	19	with	with	ADP
eurjchem-1251	184	20	naoh	naoh	NOUN
eurjchem-1251	184	21	(	(	PUNCT
eurjchem-1251	184	22	10	10	NUM
eurjchem-1251	184	23	%	%	NOUN
eurjchem-1251	184	24	)	)	PUNCT
eurjchem-1251	184	25	.	.	PUNCT
eurjchem-1251	185	1	the	the	DET
eurjchem-1251	185	2	solid	solid	ADJ
eurjchem-1251	185	3	product	product	NOUN
eurjchem-1251	185	4	was	be	AUX
eurjchem-1251	185	5	filtered	filter	VERB
eurjchem-1251	185	6	off	off	ADP
eurjchem-1251	185	7	,	,	PUNCT
eurjchem-1251	185	8	washed	wash	VERB
eurjchem-1251	185	9	with	with	ADP
eurjchem-1251	185	10	water	water	NOUN
eurjchem-1251	185	11	,	,	PUNCT
eurjchem-1251	185	12	dried	dry	VERB
eurjchem-1251	185	13	and	and	CCONJ
eurjchem-1251	185	14	recrystallized	recrystallize	VERB
eurjchem-1251	185	15	from	from	ADP
eurjchem-1251	185	16	ethanol	ethanol	NOUN
eurjchem-1251	185	17	(	(	PUNCT
eurjchem-1251	185	18	scheme	scheme	NOUN
eurjchem-1251	185	19	3	3	NUM
eurjchem-1251	185	20	)	)	PUNCT
eurjchem-1251	185	21	.	.	PUNCT
eurjchem-1251	186	1	color	color	NOUN
eurjchem-1251	186	2	:	:	PUNCT
eurjchem-1251	186	3	pale	pale	ADJ
eurjchem-1251	186	4	brown	brown	NOUN
eurjchem-1251	186	5	.	.	PUNCT
eurjchem-1251	187	1	yield	yield	NOUN
eurjchem-1251	187	2	:	:	PUNCT
eurjchem-1251	187	3	76.16	76.16	NUM
eurjchem-1251	187	4	%	%	NOUN
eurjchem-1251	187	5	.	.	PUNCT
eurjchem-1251	188	1	m.p	m.p	PROPN
eurjchem-1251	188	2	.	.	PROPN
eurjchem-1251	188	3	:	:	PUNCT
eurjchem-1251	189	1	196‐198	196‐198	PROPN
eurjchem-1251	189	2	°	°	SYM
eurjchem-1251	189	3	c	c	X
eurjchem-1251	189	4	.	.	PUNCT
eurjchem-1251	190	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	190	2	(	(	PUNCT
eurjchem-1251	190	3	kbr	kbr	PROPN
eurjchem-1251	190	4	,	,	PUNCT
eurjchem-1251	190	5	ν	ν	PROPN
eurjchem-1251	190	6	,	,	PUNCT
eurjchem-1251	190	7	cm‐1	cm‐1	PROPN
eurjchem-1251	190	8	):	):	PUNCT
eurjchem-1251	190	9	3431	3431	NUM
eurjchem-1251	190	10	,	,	PUNCT
eurjchem-1251	190	11	3389	3389	NUM
eurjchem-1251	190	12	(	(	PUNCT
eurjchem-1251	190	13	nh2	nh2	PROPN
eurjchem-1251	190	14	)	)	PUNCT
eurjchem-1251	190	15	,	,	PUNCT
eurjchem-1251	190	16	3058	3058	NUM
eurjchem-1251	190	17	(	(	PUNCT
eurjchem-1251	190	18	ch	ch	NOUN
eurjchem-1251	190	19	arom	arom	NOUN
eurjchem-1251	190	20	.	.	PUNCT
eurjchem-1251	190	21	)	)	PUNCT
eurjchem-1251	190	22	,	,	PUNCT
eurjchem-1251	190	23	1645	1645	NUM
eurjchem-1251	190	24	(	(	PUNCT
eurjchem-1251	190	25	c	c	NOUN
eurjchem-1251	190	26	=	=	NOUN
eurjchem-1251	190	27	o	o	NOUN
eurjchem-1251	190	28	amide	amide	NOUN
eurjchem-1251	190	29	)	)	PUNCT
eurjchem-1251	190	30	.	.	PUNCT
eurjchem-1251	191	1	deeb	deeb	PROPN
eurjchem-1251	191	2	et	et	PROPN
eurjchem-1251	191	3	al	al	PROPN
eurjchem-1251	191	4	.	.	PUNCT
eurjchem-1251	191	5	/	/	SYM
eurjchem-1251	191	6	european	european	PROPN
eurjchem-1251	191	7	journal	journal	PROPN
eurjchem-1251	191	8	of	of	ADP
eurjchem-1251	191	9	chemistry	chemistry	NOUN
eurjchem-1251	191	10	6	6	NUM
eurjchem-1251	191	11	(	(	PUNCT
eurjchem-1251	191	12	2	2	NUM
eurjchem-1251	191	13	)	)	PUNCT
eurjchem-1251	191	14	(	(	PUNCT
eurjchem-1251	191	15	2015	2015	NUM
eurjchem-1251	191	16	)	)	PUNCT
eurjchem-1251	191	17	211‐218	211‐218	NOUN
eurjchem-1251	191	18	215	215	NUM
eurjchem-1251	191	19	scheme	scheme	NOUN
eurjchem-1251	191	20	4	4	NUM
eurjchem-1251	191	21	1h	1h	NUM
eurjchem-1251	191	22	nmr	nmr	NOUN
eurjchem-1251	191	23	(	(	PUNCT
eurjchem-1251	191	24	300	300	NUM
eurjchem-1251	191	25	mhz	mhz	NOUN
eurjchem-1251	191	26	,	,	PUNCT
eurjchem-1251	191	27	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	191	28	,	,	PUNCT
eurjchem-1251	191	29	δ	δ	PROPN
eurjchem-1251	191	30	,	,	PUNCT
eurjchem-1251	191	31	ppm	ppm	NUM
eurjchem-1251	191	32	):	):	PUNCT
eurjchem-1251	191	33	5.49	5.49	NUM
eurjchem-1251	191	34	(	(	PUNCT
eurjchem-1251	191	35	s	s	PROPN
eurjchem-1251	191	36	,	,	PUNCT
eurjchem-1251	191	37	1h	1h	NUM
eurjchem-1251	191	38	,	,	PUNCT
eurjchem-1251	191	39	ch	ch	NOUN
eurjchem-1251	191	40	)	)	PUNCT
eurjchem-1251	191	41	,	,	PUNCT
eurjchem-1251	191	42	5.80	5.80	NUM
eurjchem-1251	191	43	(	(	PUNCT
eurjchem-1251	191	44	s	s	PROPN
eurjchem-1251	191	45	,	,	PUNCT
eurjchem-1251	191	46	2h	2h	NUM
eurjchem-1251	191	47	,	,	PUNCT
eurjchem-1251	191	48	nh2	nh2	PROPN
eurjchem-1251	191	49	)	)	PUNCT
eurjchem-1251	191	50	,	,	PUNCT
eurjchem-1251	191	51	6.89‐7.63	6.89‐7.63	NUM
eurjchem-1251	191	52	(	(	PUNCT
eurjchem-1251	191	53	m	m	PROPN
eurjchem-1251	191	54	,	,	PUNCT
eurjchem-1251	191	55	15h	15h	NUM
eurjchem-1251	191	56	,	,	PUNCT
eurjchem-1251	191	57	3ph	3ph	NOUN
eurjchem-1251	191	58	)	)	PUNCT
eurjchem-1251	191	59	.	.	PUNCT
eurjchem-1251	192	1	ms	ms	NOUN
eurjchem-1251	192	2	(	(	PUNCT
eurjchem-1251	192	3	ei	ei	PROPN
eurjchem-1251	192	4	,	,	PUNCT
eurjchem-1251	192	5	m	m	PROPN
eurjchem-1251	192	6	/	/	SYM
eurjchem-1251	192	7	z	z	PROPN
eurjchem-1251	192	8	(	(	PUNCT
eurjchem-1251	192	9	%	%	NOUN
eurjchem-1251	192	10	)	)	PUNCT
eurjchem-1251	192	11	):	):	PUNCT
eurjchem-1251	192	12	390	390	NUM
eurjchem-1251	192	13	(	(	PUNCT
eurjchem-1251	192	14	m+	m+	NUM
eurjchem-1251	192	15	,	,	PUNCT
eurjchem-1251	192	16	70.87	70.87	NUM
eurjchem-1251	192	17	)	)	PUNCT
eurjchem-1251	192	18	,	,	PUNCT
eurjchem-1251	192	19	350	350	NUM
eurjchem-1251	192	20	(	(	PUNCT
eurjchem-1251	192	21	67.96	67.96	NUM
eurjchem-1251	192	22	)	)	PUNCT
eurjchem-1251	192	23	,	,	PUNCT
eurjchem-1251	192	24	347	347	NUM
eurjchem-1251	192	25	(	(	PUNCT
eurjchem-1251	192	26	64.08	64.08	NUM
eurjchem-1251	192	27	)	)	PUNCT
eurjchem-1251	192	28	,	,	PUNCT
eurjchem-1251	192	29	335	335	NUM
eurjchem-1251	192	30	(	(	PUNCT
eurjchem-1251	192	31	52.43	52.43	NUM
eurjchem-1251	192	32	)	)	PUNCT
eurjchem-1251	192	33	,	,	PUNCT
eurjchem-1251	192	34	312	312	NUM
eurjchem-1251	192	35	(	(	PUNCT
eurjchem-1251	192	36	7.77	7.77	NUM
eurjchem-1251	192	37	)	)	PUNCT
eurjchem-1251	192	38	,	,	PUNCT
eurjchem-1251	192	39	271	271	NUM
eurjchem-1251	192	40	(	(	PUNCT
eurjchem-1251	192	41	58.25	58.25	NUM
eurjchem-1251	192	42	)	)	PUNCT
eurjchem-1251	192	43	,	,	PUNCT
eurjchem-1251	192	44	246	246	NUM
eurjchem-1251	192	45	(	(	PUNCT
eurjchem-1251	192	46	52.43	52.43	NUM
eurjchem-1251	192	47	)	)	PUNCT
eurjchem-1251	192	48	,	,	PUNCT
eurjchem-1251	192	49	236	236	NUM
eurjchem-1251	192	50	(	(	PUNCT
eurjchem-1251	192	51	58.25	58.25	NUM
eurjchem-1251	192	52	)	)	PUNCT
eurjchem-1251	192	53	,	,	PUNCT
eurjchem-1251	192	54	204	204	NUM
eurjchem-1251	192	55	(	(	PUNCT
eurjchem-1251	192	56	81.55	81.55	NUM
eurjchem-1251	192	57	)	)	PUNCT
eurjchem-1251	192	58	,	,	PUNCT
eurjchem-1251	192	59	161	161	NUM
eurjchem-1251	192	60	(	(	PUNCT
eurjchem-1251	192	61	66.02	66.02	NUM
eurjchem-1251	192	62	)	)	PUNCT
eurjchem-1251	192	63	,	,	PUNCT
eurjchem-1251	192	64	103	103	NUM
eurjchem-1251	192	65	(	(	PUNCT
eurjchem-1251	192	66	64.08	64.08	NUM
eurjchem-1251	192	67	)	)	PUNCT
eurjchem-1251	192	68	,	,	PUNCT
eurjchem-1251	192	69	79	79	NUM
eurjchem-1251	192	70	(	(	PUNCT
eurjchem-1251	192	71	100	100	NUM
eurjchem-1251	192	72	)	)	PUNCT
eurjchem-1251	192	73	,	,	PUNCT
eurjchem-1251	192	74	77	77	NUM
eurjchem-1251	192	75	(	(	PUNCT
eurjchem-1251	192	76	83.50	83.50	NUM
eurjchem-1251	192	77	)	)	PUNCT
eurjchem-1251	192	78	,	,	PUNCT
eurjchem-1251	192	79	76	76	NUM
eurjchem-1251	192	80	(	(	PUNCT
eurjchem-1251	192	81	53.40	53.40	NUM
eurjchem-1251	192	82	)	)	PUNCT
eurjchem-1251	192	83	.	.	PUNCT
eurjchem-1251	193	1	anal	anal	PROPN
eurjchem-1251	193	2	.	.	PUNCT
eurjchem-1251	193	3	calcd	calcd	NOUN
eurjchem-1251	193	4	.	.	PUNCT
eurjchem-1251	194	1	for	for	ADP
eurjchem-1251	194	2	c25h18n4o	c25h18n4o	NOUN
eurjchem-1251	194	3	:	:	PUNCT
eurjchem-1251	194	4	c	c	X
eurjchem-1251	194	5	,	,	PUNCT
eurjchem-1251	194	6	76.91	76.91	NUM
eurjchem-1251	194	7	;	;	PUNCT
eurjchem-1251	194	8	h	h	NOUN
eurjchem-1251	194	9	,	,	PUNCT
eurjchem-1251	194	10	4.65	4.65	NUM
eurjchem-1251	194	11	;	;	PUNCT
eurjchem-1251	194	12	n	n	CCONJ
eurjchem-1251	194	13	,	,	PUNCT
eurjchem-1251	194	14	14.35	14.35	NUM
eurjchem-1251	194	15	.	.	PUNCT
eurjchem-1251	194	16	found	find	VERB
eurjchem-1251	194	17	:	:	PUNCT
eurjchem-1251	195	1	c	c	X
eurjchem-1251	195	2	,	,	PUNCT
eurjchem-1251	195	3	77.40	77.40	NUM
eurjchem-1251	195	4	;	;	PUNCT
eurjchem-1251	195	5	h	h	NOUN
eurjchem-1251	195	6	,	,	PUNCT
eurjchem-1251	195	7	4.90	4.90	NUM
eurjchem-1251	195	8	;	;	PUNCT
eurjchem-1251	195	9	n	n	CCONJ
eurjchem-1251	195	10	,	,	PUNCT
eurjchem-1251	195	11	14.70	14.70	NUM
eurjchem-1251	195	12	%	%	NOUN
eurjchem-1251	195	13	.	.	PUNCT
eurjchem-1251	196	1	2.2.16	2.2.16	NUM
eurjchem-1251	196	2	.	.	PUNCT
eurjchem-1251	197	1	synthesis	synthesis	NOUN
eurjchem-1251	197	2	of	of	ADP
eurjchem-1251	197	3	4‐acetylamino‐7,8,9‐triphenyl‐2h‐	4‐acetylamino‐7,8,9‐triphenyl‐2h‐	NUM
eurjchem-1251	197	4	pyrimido[1,2‐b]pyridazin‐2‐one	pyrimido[1,2‐b]pyridazin‐2‐one	NOUN
eurjchem-1251	197	5	(	(	PUNCT
eurjchem-1251	197	6	11b	11b	NOUN
eurjchem-1251	197	7	)	)	PUNCT
eurjchem-1251	197	8	a	a	DET
eurjchem-1251	197	9	solution	solution	NOUN
eurjchem-1251	197	10	of	of	ADP
eurjchem-1251	197	11	compound	compound	NOUN
eurjchem-1251	197	12	11a	11a	NOUN
eurjchem-1251	197	13	(	(	PUNCT
eurjchem-1251	197	14	0.5	0.5	NUM
eurjchem-1251	197	15	g	g	NOUN
eurjchem-1251	197	16	,	,	PUNCT
eurjchem-1251	197	17	1.28	1.28	NUM
eurjchem-1251	197	18	mmol	mmol	NOUN
eurjchem-1251	197	19	)	)	PUNCT
eurjchem-1251	197	20	in	in	ADP
eurjchem-1251	197	21	acetic	acetic	ADJ
eurjchem-1251	197	22	anhydride	anhydride	NOUN
eurjchem-1251	197	23	(	(	PUNCT
eurjchem-1251	197	24	10	10	NUM
eurjchem-1251	197	25	ml	ml	NOUN
eurjchem-1251	197	26	)	)	PUNCT
eurjchem-1251	197	27	was	be	AUX
eurjchem-1251	197	28	refluxed	refluxe	VERB
eurjchem-1251	197	29	for	for	ADP
eurjchem-1251	197	30	3	3	NUM
eurjchem-1251	197	31	h.	h.	NOUN
eurjchem-1251	197	32	the	the	DET
eurjchem-1251	197	33	solvent	solvent	NOUN
eurjchem-1251	197	34	was	be	AUX
eurjchem-1251	197	35	then	then	ADV
eurjchem-1251	197	36	evaporated	evaporate	VERB
eurjchem-1251	197	37	under	under	ADP
eurjchem-1251	197	38	reduced	reduced	ADJ
eurjchem-1251	197	39	pressure	pressure	NOUN
eurjchem-1251	197	40	;	;	PUNCT
eurjchem-1251	197	41	the	the	DET
eurjchem-1251	197	42	solid	solid	ADJ
eurjchem-1251	197	43	product	product	NOUN
eurjchem-1251	197	44	was	be	AUX
eurjchem-1251	197	45	collected	collect	VERB
eurjchem-1251	197	46	and	and	CCONJ
eurjchem-1251	197	47	recrystallized	recrystallize	VERB
eurjchem-1251	197	48	from	from	ADP
eurjchem-1251	197	49	acetone	acetone	NOUN
eurjchem-1251	197	50	(	(	PUNCT
eurjchem-1251	197	51	scheme	scheme	NOUN
eurjchem-1251	197	52	3	3	NUM
eurjchem-1251	197	53	)	)	PUNCT
eurjchem-1251	197	54	.	.	PUNCT
eurjchem-1251	198	1	color	color	NOUN
eurjchem-1251	198	2	:	:	PUNCT
eurjchem-1251	198	3	dark	dark	PROPN
eurjchem-1251	198	4	brown	brown	PROPN
eurjchem-1251	198	5	.	.	PUNCT
eurjchem-1251	199	1	yield	yield	NOUN
eurjchem-1251	199	2	:	:	PUNCT
eurjchem-1251	199	3	79.57	79.57	NUM
eurjchem-1251	199	4	%	%	NOUN
eurjchem-1251	199	5	.	.	PUNCT
eurjchem-1251	200	1	m.p	m.p	PROPN
eurjchem-1251	200	2	.	.	PROPN
eurjchem-1251	200	3	:	:	PUNCT
eurjchem-1251	201	1	>	>	X
eurjchem-1251	201	2	300	300	NUM
eurjchem-1251	201	3	°	°	SYM
eurjchem-1251	201	4	c	c	NOUN
eurjchem-1251	201	5	.	.	PUNCT
eurjchem-1251	202	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	202	2	(	(	PUNCT
eurjchem-1251	202	3	kbr	kbr	PROPN
eurjchem-1251	202	4	,	,	PUNCT
eurjchem-1251	202	5	ν	ν	PROPN
eurjchem-1251	202	6	,	,	PUNCT
eurjchem-1251	202	7	cm‐	cm‐	NOUN
eurjchem-1251	202	8	1	1	NUM
eurjchem-1251	202	9	):	):	PUNCT
eurjchem-1251	202	10	3357	3357	NUM
eurjchem-1251	202	11	(	(	PUNCT
eurjchem-1251	202	12	nh	nh	NOUN
eurjchem-1251	202	13	amide	amide	NOUN
eurjchem-1251	202	14	)	)	PUNCT
eurjchem-1251	202	15	,	,	PUNCT
eurjchem-1251	202	16	3059	3059	NUM
eurjchem-1251	202	17	(	(	PUNCT
eurjchem-1251	202	18	ch	ch	NOUN
eurjchem-1251	202	19	arom	arom	NOUN
eurjchem-1251	202	20	.	.	PUNCT
eurjchem-1251	202	21	)	)	PUNCT
eurjchem-1251	202	22	,	,	PUNCT
eurjchem-1251	202	23	2979	2979	NUM
eurjchem-1251	202	24	,	,	PUNCT
eurjchem-1251	202	25	2932	2932	NUM
eurjchem-1251	202	26	(	(	PUNCT
eurjchem-1251	202	27	ch	ch	NOUN
eurjchem-1251	202	28	aliph	aliph	PROPN
eurjchem-1251	202	29	.	.	PUNCT
eurjchem-1251	202	30	)	)	PUNCT
eurjchem-1251	202	31	,	,	PUNCT
eurjchem-1251	202	32	1700	1700	NUM
eurjchem-1251	202	33	(	(	PUNCT
eurjchem-1251	202	34	c	c	NOUN
eurjchem-1251	202	35	=	=	NOUN
eurjchem-1251	202	36	o	o	NOUN
eurjchem-1251	202	37	cyclic	cyclic	NOUN
eurjchem-1251	202	38	)	)	PUNCT
eurjchem-1251	202	39	,	,	PUNCT
eurjchem-1251	202	40	1634	1634	NUM
eurjchem-1251	202	41	(	(	PUNCT
eurjchem-1251	202	42	c	c	NOUN
eurjchem-1251	202	43	=	=	NOUN
eurjchem-1251	202	44	o	o	NOUN
eurjchem-1251	202	45	amide	amide	NOUN
eurjchem-1251	202	46	)	)	PUNCT
eurjchem-1251	202	47	.	.	PUNCT
eurjchem-1251	203	1	1h	1h	NUM
eurjchem-1251	203	2	nmr	nmr	NOUN
eurjchem-1251	203	3	(	(	PUNCT
eurjchem-1251	203	4	300	300	NUM
eurjchem-1251	203	5	mhz	mhz	NOUN
eurjchem-1251	203	6	,	,	PUNCT
eurjchem-1251	203	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	203	8	,	,	PUNCT
eurjchem-1251	203	9	δ	δ	PROPN
eurjchem-1251	203	10	,	,	PUNCT
eurjchem-1251	203	11	ppm	ppm	NUM
eurjchem-1251	203	12	):	):	PUNCT
eurjchem-1251	203	13	1.80	1.80	NUM
eurjchem-1251	203	14	(	(	PUNCT
eurjchem-1251	203	15	s	s	PROPN
eurjchem-1251	203	16	,	,	PUNCT
eurjchem-1251	203	17	3h	3h	NUM
eurjchem-1251	203	18	,	,	PUNCT
eurjchem-1251	203	19	ch3	ch3	PROPN
eurjchem-1251	203	20	)	)	PUNCT
eurjchem-1251	203	21	,	,	PUNCT
eurjchem-1251	203	22	6.56	6.56	NUM
eurjchem-1251	203	23	(	(	PUNCT
eurjchem-1251	203	24	s	s	PROPN
eurjchem-1251	203	25	,	,	PUNCT
eurjchem-1251	203	26	1h	1h	NUM
eurjchem-1251	203	27	,	,	PUNCT
eurjchem-1251	203	28	h‐3	h‐3	NOUN
eurjchem-1251	203	29	)	)	PUNCT
eurjchem-1251	203	30	,	,	PUNCT
eurjchem-1251	203	31	7.70	7.70	NUM
eurjchem-1251	203	32	(	(	PUNCT
eurjchem-1251	203	33	d	d	PROPN
eurjchem-1251	203	34	,	,	PUNCT
eurjchem-1251	203	35	1h	1h	NUM
eurjchem-1251	203	36	,	,	PUNCT
eurjchem-1251	203	37	nh	nh	PROPN
eurjchem-1251	203	38	)	)	PUNCT
eurjchem-1251	203	39	,	,	PUNCT
eurjchem-1251	203	40	7.29‐7.98	7.29‐7.98	NUM
eurjchem-1251	203	41	(	(	PUNCT
eurjchem-1251	203	42	m	m	PROPN
eurjchem-1251	203	43	,	,	PUNCT
eurjchem-1251	203	44	15h	15h	NUM
eurjchem-1251	203	45	,	,	PUNCT
eurjchem-1251	203	46	3ph	3ph	NOUN
eurjchem-1251	203	47	)	)	PUNCT
eurjchem-1251	203	48	.	.	PUNCT
eurjchem-1251	204	1	ms	ms	NOUN
eurjchem-1251	204	2	(	(	PUNCT
eurjchem-1251	204	3	ei	ei	PROPN
eurjchem-1251	204	4	,	,	PUNCT
eurjchem-1251	204	5	m	m	PROPN
eurjchem-1251	204	6	/	/	SYM
eurjchem-1251	204	7	z	z	PROPN
eurjchem-1251	204	8	(	(	PUNCT
eurjchem-1251	204	9	%	%	NOUN
eurjchem-1251	204	10	)	)	PUNCT
eurjchem-1251	204	11	):	):	PUNCT
eurjchem-1251	204	12	432	432	NUM
eurjchem-1251	204	13	(	(	PUNCT
eurjchem-1251	204	14	m+	m+	NUM
eurjchem-1251	204	15	,	,	PUNCT
eurjchem-1251	204	16	14.40	14.40	NUM
eurjchem-1251	204	17	)	)	PUNCT
eurjchem-1251	204	18	,	,	PUNCT
eurjchem-1251	204	19	377	377	NUM
eurjchem-1251	204	20	(	(	PUNCT
eurjchem-1251	204	21	23.25	23.25	NUM
eurjchem-1251	204	22	)	)	PUNCT
eurjchem-1251	204	23	,	,	PUNCT
eurjchem-1251	204	24	372	372	NUM
eurjchem-1251	204	25	(	(	PUNCT
eurjchem-1251	204	26	12.96	12.96	NUM
eurjchem-1251	204	27	)	)	PUNCT
eurjchem-1251	204	28	,	,	PUNCT
eurjchem-1251	204	29	353	353	NUM
eurjchem-1251	204	30	(	(	PUNCT
eurjchem-1251	204	31	11.73	11.73	NUM
eurjchem-1251	204	32	)	)	PUNCT
eurjchem-1251	204	33	,	,	PUNCT
eurjchem-1251	204	34	350	350	NUM
eurjchem-1251	204	35	(	(	PUNCT
eurjchem-1251	204	36	13.37	13.37	NUM
eurjchem-1251	204	37	)	)	PUNCT
eurjchem-1251	204	38	,	,	PUNCT
eurjchem-1251	204	39	328	328	NUM
eurjchem-1251	204	40	(	(	PUNCT
eurjchem-1251	204	41	12.76	12.76	NUM
eurjchem-1251	204	42	)	)	PUNCT
eurjchem-1251	204	43	,	,	PUNCT
eurjchem-1251	204	44	314	314	NUM
eurjchem-1251	204	45	(	(	PUNCT
eurjchem-1251	204	46	11.32	11.32	NUM
eurjchem-1251	204	47	)	)	PUNCT
eurjchem-1251	204	48	,	,	PUNCT
eurjchem-1251	204	49	305	305	NUM
eurjchem-1251	204	50	(	(	PUNCT
eurjchem-1251	204	51	10.70	10.70	NUM
eurjchem-1251	204	52	)	)	PUNCT
eurjchem-1251	204	53	,	,	PUNCT
eurjchem-1251	204	54	227	227	NUM
eurjchem-1251	204	55	(	(	PUNCT
eurjchem-1251	204	56	16.87	16.87	NUM
eurjchem-1251	204	57	)	)	PUNCT
eurjchem-1251	204	58	,	,	PUNCT
eurjchem-1251	204	59	205	205	NUM
eurjchem-1251	204	60	(	(	PUNCT
eurjchem-1251	204	61	23.87	23.87	NUM
eurjchem-1251	204	62	)	)	PUNCT
eurjchem-1251	204	63	,	,	PUNCT
eurjchem-1251	204	64	125	125	NUM
eurjchem-1251	204	65	(	(	PUNCT
eurjchem-1251	204	66	11.73	11.73	NUM
eurjchem-1251	204	67	)	)	PUNCT
eurjchem-1251	204	68	,	,	PUNCT
eurjchem-1251	204	69	117	117	NUM
eurjchem-1251	204	70	(	(	PUNCT
eurjchem-1251	204	71	16.05	16.05	NUM
eurjchem-1251	204	72	)	)	PUNCT
eurjchem-1251	204	73	,	,	PUNCT
eurjchem-1251	204	74	102	102	NUM
eurjchem-1251	204	75	(	(	PUNCT
eurjchem-1251	204	76	14.61	14.61	NUM
eurjchem-1251	204	77	)	)	PUNCT
eurjchem-1251	204	78	,	,	PUNCT
eurjchem-1251	204	79	84	84	NUM
eurjchem-1251	204	80	(	(	PUNCT
eurjchem-1251	204	81	14.61	14.61	NUM
eurjchem-1251	204	82	)	)	PUNCT
eurjchem-1251	204	83	,	,	PUNCT
eurjchem-1251	204	84	80	80	NUM
eurjchem-1251	204	85	(	(	PUNCT
eurjchem-1251	204	86	100	100	NUM
eurjchem-1251	204	87	)	)	PUNCT
eurjchem-1251	204	88	,	,	PUNCT
eurjchem-1251	204	89	59	59	NUM
eurjchem-1251	204	90	(	(	PUNCT
eurjchem-1251	204	91	14.40	14.40	NUM
eurjchem-1251	204	92	)	)	PUNCT
eurjchem-1251	204	93	,	,	PUNCT
eurjchem-1251	204	94	53	53	NUM
eurjchem-1251	204	95	(	(	PUNCT
eurjchem-1251	204	96	16.67	16.67	NUM
eurjchem-1251	204	97	)	)	PUNCT
eurjchem-1251	204	98	.	.	PUNCT
eurjchem-1251	205	1	anal	anal	PROPN
eurjchem-1251	205	2	.	.	PUNCT
eurjchem-1251	205	3	calcd	calcd	NOUN
eurjchem-1251	205	4	.	.	PUNCT
eurjchem-1251	206	1	for	for	SCONJ
eurjchem-1251	206	2	c27h20n4o2	c27h20n4o2	PROPN
eurjchem-1251	206	3	:	:	PUNCT
eurjchem-1251	206	4	c	c	X
eurjchem-1251	206	5	,	,	PUNCT
eurjchem-1251	206	6	74.98	74.98	NUM
eurjchem-1251	206	7	;	;	PUNCT
eurjchem-1251	206	8	h	h	NOUN
eurjchem-1251	206	9	,	,	PUNCT
eurjchem-1251	206	10	4.66	4.66	NUM
eurjchem-1251	206	11	;	;	PUNCT
eurjchem-1251	206	12	n	n	CCONJ
eurjchem-1251	206	13	,	,	PUNCT
eurjchem-1251	206	14	12.95	12.95	NUM
eurjchem-1251	206	15	.	.	PUNCT
eurjchem-1251	206	16	found	find	VERB
eurjchem-1251	206	17	:	:	PUNCT
eurjchem-1251	207	1	c	c	X
eurjchem-1251	207	2	,	,	PUNCT
eurjchem-1251	207	3	74.70	74.70	NUM
eurjchem-1251	207	4	;	;	PUNCT
eurjchem-1251	208	1	h	h	NOUN
eurjchem-1251	208	2	,	,	PUNCT
eurjchem-1251	208	3	4.60	4.60	NUM
eurjchem-1251	208	4	;	;	PUNCT
eurjchem-1251	208	5	n	n	CCONJ
eurjchem-1251	208	6	,	,	PUNCT
eurjchem-1251	208	7	12.70	12.70	NUM
eurjchem-1251	208	8	%	%	NOUN
eurjchem-1251	208	9	.	.	PUNCT
eurjchem-1251	209	1	2.2.17	2.2.17	X
eurjchem-1251	209	2	.	.	PUNCT
eurjchem-1251	209	3	synthesis	synthesis	NOUN
eurjchem-1251	209	4	of	of	ADP
eurjchem-1251	209	5	ethyl	ethyl	PROPN
eurjchem-1251	209	6	3‐[(4,5,6‐triphenylpyridazin‐3‐yl	3‐[(4,5,6‐triphenylpyridazin‐3‐yl	NUM
eurjchem-1251	209	7	)	)	PUNCT
eurjchem-1251	209	8	imino]butanoate	imino]butanoate	PROPN
eurjchem-1251	209	9	(	(	PUNCT
eurjchem-1251	209	10	12a	12a	NOUN
eurjchem-1251	209	11	)	)	PUNCT
eurjchem-1251	209	12	a	a	DET
eurjchem-1251	209	13	mixture	mixture	NOUN
eurjchem-1251	209	14	of	of	ADP
eurjchem-1251	209	15	compound	compound	NOUN
eurjchem-1251	209	16	5	5	NUM
eurjchem-1251	209	17	(	(	PUNCT
eurjchem-1251	209	18	0.5	0.5	NUM
eurjchem-1251	209	19	g	g	NOUN
eurjchem-1251	209	20	,	,	PUNCT
eurjchem-1251	209	21	1.55	1.55	NUM
eurjchem-1251	209	22	mmol	mmol	NOUN
eurjchem-1251	209	23	)	)	PUNCT
eurjchem-1251	209	24	and	and	CCONJ
eurjchem-1251	209	25	ethyl	ethyl	PROPN
eurjchem-1251	209	26	acetoacetate	acetoacetate	NOUN
eurjchem-1251	209	27	(	(	PUNCT
eurjchem-1251	209	28	0.2	0.2	NUM
eurjchem-1251	209	29	ml	ml	NOUN
eurjchem-1251	209	30	,	,	PUNCT
eurjchem-1251	209	31	1.55	1.55	NUM
eurjchem-1251	209	32	mmol	mmol	NOUN
eurjchem-1251	209	33	)	)	PUNCT
eurjchem-1251	209	34	was	be	AUX
eurjchem-1251	209	35	heated	heat	VERB
eurjchem-1251	209	36	under	under	ADP
eurjchem-1251	209	37	reflux	reflux	NOUN
eurjchem-1251	209	38	for	for	ADP
eurjchem-1251	209	39	3	3	NUM
eurjchem-1251	209	40	h.	h.	NOUN
eurjchem-1251	209	41	after	after	ADP
eurjchem-1251	209	42	cooling	cool	VERB
eurjchem-1251	209	43	,	,	PUNCT
eurjchem-1251	209	44	the	the	DET
eurjchem-1251	209	45	reaction	reaction	NOUN
eurjchem-1251	209	46	mixture	mixture	NOUN
eurjchem-1251	209	47	was	be	AUX
eurjchem-1251	209	48	treated	treat	VERB
eurjchem-1251	209	49	with	with	ADP
eurjchem-1251	209	50	diethyl	diethyl	NOUN
eurjchem-1251	209	51	ether	ether	NOUN
eurjchem-1251	209	52	(	(	PUNCT
eurjchem-1251	209	53	50	50	NUM
eurjchem-1251	209	54	ml	ml	NOUN
eurjchem-1251	209	55	)	)	PUNCT
eurjchem-1251	209	56	,	,	PUNCT
eurjchem-1251	209	57	and	and	CCONJ
eurjchem-1251	209	58	the	the	DET
eurjchem-1251	209	59	solid	solid	ADJ
eurjchem-1251	209	60	product	product	NOUN
eurjchem-1251	209	61	formed	form	VERB
eurjchem-1251	209	62	was	be	AUX
eurjchem-1251	209	63	filtered	filter	VERB
eurjchem-1251	209	64	off	off	ADP
eurjchem-1251	209	65	,	,	PUNCT
eurjchem-1251	209	66	dried	dry	VERB
eurjchem-1251	209	67	and	and	CCONJ
eurjchem-1251	209	68	recrystallized	recrystallize	VERB
eurjchem-1251	209	69	from	from	ADP
eurjchem-1251	209	70	ethanol	ethanol	NOUN
eurjchem-1251	209	71	(	(	PUNCT
eurjchem-1251	209	72	scheme	scheme	NOUN
eurjchem-1251	209	73	3	3	NUM
eurjchem-1251	209	74	)	)	PUNCT
eurjchem-1251	209	75	.	.	PUNCT
eurjchem-1251	210	1	color	color	NOUN
eurjchem-1251	210	2	:	:	PUNCT
eurjchem-1251	210	3	brown	brown	ADJ
eurjchem-1251	210	4	.	.	PUNCT
eurjchem-1251	211	1	yield	yield	NOUN
eurjchem-1251	211	2	:	:	PUNCT
eurjchem-1251	211	3	77.22	77.22	NUM
eurjchem-1251	211	4	%	%	NOUN
eurjchem-1251	211	5	.	.	PUNCT
eurjchem-1251	212	1	m.p	m.p	PROPN
eurjchem-1251	212	2	.	.	PROPN
eurjchem-1251	212	3	:	:	PUNCT
eurjchem-1251	213	1	216‐218	216‐218	NUM
eurjchem-1251	213	2	°	°	SYM
eurjchem-1251	213	3	c	c	X
eurjchem-1251	213	4	.	.	PUNCT
eurjchem-1251	214	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	214	2	(	(	PUNCT
eurjchem-1251	214	3	kbr	kbr	PROPN
eurjchem-1251	214	4	,	,	PUNCT
eurjchem-1251	214	5	ν	ν	PROPN
eurjchem-1251	214	6	,	,	PUNCT
eurjchem-1251	214	7	cm‐1	cm‐1	PROPN
eurjchem-1251	214	8	):	):	PUNCT
eurjchem-1251	214	9	3057	3057	NUM
eurjchem-1251	214	10	(	(	PUNCT
eurjchem-1251	214	11	ch	ch	NOUN
eurjchem-1251	214	12	arom	arom	NOUN
eurjchem-1251	214	13	.	.	PUNCT
eurjchem-1251	214	14	)	)	PUNCT
eurjchem-1251	214	15	,	,	PUNCT
eurjchem-1251	214	16	2977	2977	NUM
eurjchem-1251	214	17	,	,	PUNCT
eurjchem-1251	214	18	2927	2927	NUM
eurjchem-1251	214	19	(	(	PUNCT
eurjchem-1251	214	20	ch	ch	NOUN
eurjchem-1251	214	21	aliph	aliph	PROPN
eurjchem-1251	214	22	.	.	PUNCT
eurjchem-1251	214	23	)	)	PUNCT
eurjchem-1251	214	24	,	,	PUNCT
eurjchem-1251	214	25	1718	1718	NUM
eurjchem-1251	214	26	(	(	PUNCT
eurjchem-1251	214	27	c	c	NOUN
eurjchem-1251	214	28	=	=	NOUN
eurjchem-1251	214	29	o	o	NOUN
eurjchem-1251	214	30	ester	ester	NOUN
eurjchem-1251	214	31	)	)	PUNCT
eurjchem-1251	214	32	,	,	PUNCT
eurjchem-1251	214	33	1650	1650	NUM
eurjchem-1251	214	34	(	(	PUNCT
eurjchem-1251	214	35	c	c	NOUN
eurjchem-1251	214	36	=	=	NOUN
eurjchem-1251	214	37	n	n	PRON
eurjchem-1251	214	38	imino	imino	NOUN
eurjchem-1251	214	39	)	)	PUNCT
eurjchem-1251	214	40	,	,	PUNCT
eurjchem-1251	214	41	1231	1231	NUM
eurjchem-1251	214	42	(	(	PUNCT
eurjchem-1251	214	43	c‐o	c‐o	NOUN
eurjchem-1251	214	44	acetate	acetate	NOUN
eurjchem-1251	214	45	)	)	PUNCT
eurjchem-1251	214	46	.	.	PUNCT
eurjchem-1251	215	1	1h	1h	NUM
eurjchem-1251	215	2	nmr	nmr	NOUN
eurjchem-1251	215	3	(	(	PUNCT
eurjchem-1251	215	4	300	300	NUM
eurjchem-1251	215	5	mhz	mhz	NOUN
eurjchem-1251	215	6	,	,	PUNCT
eurjchem-1251	215	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	215	8	,	,	PUNCT
eurjchem-1251	215	9	δ	δ	PROPN
eurjchem-1251	215	10	,	,	PUNCT
eurjchem-1251	215	11	ppm	ppm	NUM
eurjchem-1251	215	12	):	):	PUNCT
eurjchem-1251	215	13	2.8	2.8	NUM
eurjchem-1251	215	14	(	(	PUNCT
eurjchem-1251	215	15	t	t	PROPN
eurjchem-1251	215	16	,	,	PUNCT
eurjchem-1251	215	17	j	j	PROPN
eurjchem-1251	215	18	=	=	SYM
eurjchem-1251	215	19	7.5	7.5	NUM
eurjchem-1251	215	20	hz	hz	NOUN
eurjchem-1251	215	21	,	,	PUNCT
eurjchem-1251	215	22	3h	3h	NUM
eurjchem-1251	215	23	,	,	PUNCT
eurjchem-1251	215	24	ch2ch3	ch2ch3	ADJ
eurjchem-1251	215	25	)	)	PUNCT
eurjchem-1251	215	26	,	,	PUNCT
eurjchem-1251	215	27	1.91	1.91	NUM
eurjchem-1251	215	28	(	(	PUNCT
eurjchem-1251	215	29	s	s	PROPN
eurjchem-1251	215	30	,	,	PUNCT
eurjchem-1251	215	31	3h	3h	NUM
eurjchem-1251	215	32	,	,	PUNCT
eurjchem-1251	215	33	ch3c	ch3c	NOUN
eurjchem-1251	215	34	=	=	SYM
eurjchem-1251	215	35	n	n	NUM
eurjchem-1251	215	36	)	)	PUNCT
eurjchem-1251	215	37	,	,	PUNCT
eurjchem-1251	215	38	2.60	2.60	NUM
eurjchem-1251	215	39	(	(	PUNCT
eurjchem-1251	215	40	s	s	PROPN
eurjchem-1251	215	41	,	,	PUNCT
eurjchem-1251	215	42	2h	2h	NUM
eurjchem-1251	215	43	,	,	PUNCT
eurjchem-1251	215	44	ch2co	ch2co	NOUN
eurjchem-1251	215	45	)	)	PUNCT
eurjchem-1251	215	46	,	,	PUNCT
eurjchem-1251	215	47	3.83	3.83	NUM
eurjchem-1251	215	48	(	(	PUNCT
eurjchem-1251	215	49	q	q	NOUN
eurjchem-1251	215	50	,	,	PUNCT
eurjchem-1251	215	51	2h	2h	NUM
eurjchem-1251	215	52	,	,	PUNCT
eurjchem-1251	215	53	ch2ch3	ch2ch3	ADJ
eurjchem-1251	215	54	)	)	PUNCT
eurjchem-1251	215	55	,	,	PUNCT
eurjchem-1251	215	56	6.95‐	6.95‐	NUM
eurjchem-1251	215	57	7.63	7.63	NUM
eurjchem-1251	215	58	(	(	PUNCT
eurjchem-1251	215	59	m	m	PROPN
eurjchem-1251	215	60	,	,	PUNCT
eurjchem-1251	215	61	15h	15h	NUM
eurjchem-1251	215	62	,	,	PUNCT
eurjchem-1251	215	63	3ph	3ph	NOUN
eurjchem-1251	215	64	)	)	PUNCT
eurjchem-1251	215	65	.	.	PUNCT
eurjchem-1251	216	1	ms	ms	NOUN
eurjchem-1251	216	2	(	(	PUNCT
eurjchem-1251	216	3	ei	ei	PROPN
eurjchem-1251	216	4	,	,	PUNCT
eurjchem-1251	216	5	m	m	PROPN
eurjchem-1251	216	6	/	/	SYM
eurjchem-1251	216	7	z	z	PROPN
eurjchem-1251	216	8	(	(	PUNCT
eurjchem-1251	216	9	%	%	NOUN
eurjchem-1251	216	10	)	)	PUNCT
eurjchem-1251	216	11	):	):	PUNCT
eurjchem-1251	216	12	435	435	NUM
eurjchem-1251	216	13	(	(	PUNCT
eurjchem-1251	216	14	m+	m+	NUM
eurjchem-1251	216	15	,	,	PUNCT
eurjchem-1251	216	16	23.09	23.09	NUM
eurjchem-1251	216	17	)	)	PUNCT
eurjchem-1251	216	18	,	,	PUNCT
eurjchem-1251	216	19	390	390	NUM
eurjchem-1251	216	20	(	(	PUNCT
eurjchem-1251	216	21	44.86	44.86	NUM
eurjchem-1251	216	22	)	)	PUNCT
eurjchem-1251	216	23	,	,	PUNCT
eurjchem-1251	216	24	361	361	NUM
eurjchem-1251	216	25	(	(	PUNCT
eurjchem-1251	216	26	17.00	17.00	NUM
eurjchem-1251	216	27	)	)	PUNCT
eurjchem-1251	216	28	,	,	PUNCT
eurjchem-1251	216	29	358	358	NUM
eurjchem-1251	216	30	(	(	PUNCT
eurjchem-1251	216	31	19.57	19.57	NUM
eurjchem-1251	216	32	)	)	PUNCT
eurjchem-1251	216	33	,	,	PUNCT
eurjchem-1251	216	34	349	349	NUM
eurjchem-1251	216	35	(	(	PUNCT
eurjchem-1251	216	36	22.15	22.15	NUM
eurjchem-1251	216	37	)	)	PUNCT
eurjchem-1251	216	38	,	,	PUNCT
eurjchem-1251	216	39	322	322	NUM
eurjchem-1251	216	40	(	(	PUNCT
eurjchem-1251	216	41	52.64	52.64	NUM
eurjchem-1251	216	42	)	)	PUNCT
eurjchem-1251	216	43	,	,	PUNCT
eurjchem-1251	216	44	307	307	NUM
eurjchem-1251	216	45	(	(	PUNCT
eurjchem-1251	216	46	52.67	52.67	NUM
eurjchem-1251	216	47	)	)	PUNCT
eurjchem-1251	216	48	,	,	PUNCT
eurjchem-1251	216	49	256	256	NUM
eurjchem-1251	216	50	(	(	PUNCT
eurjchem-1251	216	51	13.28	13.28	NUM
eurjchem-1251	216	52	)	)	PUNCT
eurjchem-1251	216	53	,	,	PUNCT
eurjchem-1251	216	54	229	229	NUM
eurjchem-1251	216	55	(	(	PUNCT
eurjchem-1251	216	56	13.43	13.43	NUM
eurjchem-1251	216	57	)	)	PUNCT
eurjchem-1251	216	58	,	,	PUNCT
eurjchem-1251	216	59	206	206	NUM
eurjchem-1251	216	60	(	(	PUNCT
eurjchem-1251	216	61	49.44	49.44	NUM
eurjchem-1251	216	62	)	)	PUNCT
eurjchem-1251	216	63	,	,	PUNCT
eurjchem-1251	216	64	178	178	NUM
eurjchem-1251	216	65	(	(	PUNCT
eurjchem-1251	216	66	18.91	18.91	NUM
eurjchem-1251	216	67	)	)	PUNCT
eurjchem-1251	216	68	,	,	PUNCT
eurjchem-1251	216	69	176	176	NUM
eurjchem-1251	216	70	(	(	PUNCT
eurjchem-1251	216	71	100	100	NUM
eurjchem-1251	216	72	)	)	PUNCT
eurjchem-1251	216	73	,	,	PUNCT
eurjchem-1251	216	74	128	128	NUM
eurjchem-1251	216	75	(	(	PUNCT
eurjchem-1251	216	76	29.51	29.51	NUM
eurjchem-1251	216	77	)	)	PUNCT
eurjchem-1251	216	78	,	,	PUNCT
eurjchem-1251	216	79	98	98	NUM
eurjchem-1251	216	80	(	(	PUNCT
eurjchem-1251	216	81	8.46	8.46	NUM
eurjchem-1251	216	82	)	)	PUNCT
eurjchem-1251	216	83	,	,	PUNCT
eurjchem-1251	216	84	87	87	NUM
eurjchem-1251	216	85	(	(	PUNCT
eurjchem-1251	216	86	26.46	26.46	NUM
eurjchem-1251	216	87	)	)	PUNCT
eurjchem-1251	216	88	,	,	PUNCT
eurjchem-1251	216	89	74	74	NUM
eurjchem-1251	216	90	(	(	PUNCT
eurjchem-1251	216	91	22.10	22.10	NUM
eurjchem-1251	216	92	)	)	PUNCT
eurjchem-1251	216	93	.	.	PUNCT
eurjchem-1251	217	1	anal	anal	PROPN
eurjchem-1251	217	2	.	.	PUNCT
eurjchem-1251	217	3	calcd	calcd	NOUN
eurjchem-1251	217	4	.	.	PUNCT
eurjchem-1251	218	1	for	for	ADP
eurjchem-1251	218	2	c28h25n3o2	c28h25n3o2	PROPN
eurjchem-1251	218	3	:	:	PUNCT
eurjchem-1251	218	4	c	c	X
eurjchem-1251	218	5	,	,	PUNCT
eurjchem-1251	218	6	77.22	77.22	NUM
eurjchem-1251	218	7	;	;	PUNCT
eurjchem-1251	218	8	h	h	NOUN
eurjchem-1251	218	9	,	,	PUNCT
eurjchem-1251	218	10	5.79	5.79	NUM
eurjchem-1251	218	11	;	;	PUNCT
eurjchem-1251	218	12	n	n	CCONJ
eurjchem-1251	218	13	,	,	PUNCT
eurjchem-1251	218	14	9.65	9.65	NUM
eurjchem-1251	218	15	.	.	PUNCT
eurjchem-1251	218	16	found	find	VERB
eurjchem-1251	218	17	:	:	PUNCT
eurjchem-1251	219	1	c	c	X
eurjchem-1251	219	2	,	,	PUNCT
eurjchem-1251	219	3	77.60	77.60	NUM
eurjchem-1251	219	4	;	;	PUNCT
eurjchem-1251	219	5	h	h	NOUN
eurjchem-1251	219	6	,	,	PUNCT
eurjchem-1251	219	7	6.00	6.00	NUM
eurjchem-1251	219	8	;	;	PUNCT
eurjchem-1251	219	9	n	n	CCONJ
eurjchem-1251	219	10	,	,	PUNCT
eurjchem-1251	219	11	10.00	10.00	NUM
eurjchem-1251	219	12	%	%	NOUN
eurjchem-1251	219	13	.	.	PUNCT
eurjchem-1251	220	1	2.2.18	2.2.18	NUM
eurjchem-1251	220	2	.	.	PUNCT
eurjchem-1251	220	3	synthesis	synthesis	NOUN
eurjchem-1251	220	4	of	of	ADP
eurjchem-1251	220	5	3‐[(4,5,6‐triphenylpyridazin‐3‐yl)imino	3‐[(4,5,6‐triphenylpyridazin‐3‐yl)imino	NUM
eurjchem-1251	220	6	]	]	PUNCT
eurjchem-1251	220	7	butanoic	butanoic	NOUN
eurjchem-1251	220	8	acid	acid	NOUN
eurjchem-1251	220	9	(	(	PUNCT
eurjchem-1251	220	10	12b	12b	X
eurjchem-1251	220	11	)	)	PUNCT
eurjchem-1251	220	12	compound	compound	NOUN
eurjchem-1251	220	13	12a	12a	NOUN
eurjchem-1251	220	14	(	(	PUNCT
eurjchem-1251	220	15	0.5	0.5	NUM
eurjchem-1251	220	16	g	g	NOUN
eurjchem-1251	220	17	,	,	PUNCT
eurjchem-1251	220	18	1.15	1.15	NUM
eurjchem-1251	220	19	mmol	mmol	NOUN
eurjchem-1251	220	20	)	)	PUNCT
eurjchem-1251	220	21	was	be	AUX
eurjchem-1251	220	22	added	add	VERB
eurjchem-1251	220	23	to	to	ADP
eurjchem-1251	220	24	a	a	DET
eurjchem-1251	220	25	solution	solution	NOUN
eurjchem-1251	220	26	of	of	ADP
eurjchem-1251	220	27	potassium	potassium	NOUN
eurjchem-1251	220	28	hydroxide	hydroxide	NOUN
eurjchem-1251	220	29	(	(	PUNCT
eurjchem-1251	220	30	1	1	NUM
eurjchem-1251	220	31	g	g	NOUN
eurjchem-1251	220	32	)	)	PUNCT
eurjchem-1251	220	33	in	in	ADP
eurjchem-1251	220	34	ethanol	ethanol	NOUN
eurjchem-1251	220	35	(	(	PUNCT
eurjchem-1251	220	36	10	10	NUM
eurjchem-1251	220	37	ml	ml	NOUN
eurjchem-1251	220	38	)	)	PUNCT
eurjchem-1251	220	39	,	,	PUNCT
eurjchem-1251	220	40	then	then	ADV
eurjchem-1251	220	41	the	the	DET
eurjchem-1251	220	42	reaction	reaction	NOUN
eurjchem-1251	220	43	mixture	mixture	NOUN
eurjchem-1251	220	44	was	be	AUX
eurjchem-1251	220	45	heated	heat	VERB
eurjchem-1251	220	46	under	under	ADP
eurjchem-1251	220	47	reflux	reflux	NOUN
eurjchem-1251	220	48	for	for	ADP
eurjchem-1251	220	49	2	2	NUM
eurjchem-1251	220	50	h.	h.	NOUN
eurjchem-1251	220	51	after	after	ADP
eurjchem-1251	220	52	cooling	cool	VERB
eurjchem-1251	220	53	,	,	PUNCT
eurjchem-1251	220	54	the	the	DET
eurjchem-1251	220	55	reaction	reaction	NOUN
eurjchem-1251	220	56	mixture	mixture	NOUN
eurjchem-1251	220	57	was	be	AUX
eurjchem-1251	220	58	poured	pour	VERB
eurjchem-1251	220	59	into	into	ADP
eurjchem-1251	220	60	ice	ice	NOUN
eurjchem-1251	220	61	water	water	NOUN
eurjchem-1251	220	62	(	(	PUNCT
eurjchem-1251	220	63	100	100	NUM
eurjchem-1251	220	64	ml	ml	NOUN
eurjchem-1251	220	65	)	)	PUNCT
eurjchem-1251	220	66	,	,	PUNCT
eurjchem-1251	220	67	and	and	CCONJ
eurjchem-1251	220	68	neutralized	neutralize	VERB
eurjchem-1251	220	69	with	with	ADP
eurjchem-1251	220	70	hydrochloric	hydrochloric	ADJ
eurjchem-1251	220	71	acid	acid	NOUN
eurjchem-1251	220	72	.	.	PUNCT
eurjchem-1251	221	1	the	the	DET
eurjchem-1251	221	2	solid	solid	ADJ
eurjchem-1251	221	3	product	product	NOUN
eurjchem-1251	221	4	was	be	AUX
eurjchem-1251	221	5	filtered	filter	VERB
eurjchem-1251	221	6	off	off	ADP
eurjchem-1251	221	7	,	,	PUNCT
eurjchem-1251	221	8	washed	wash	VERB
eurjchem-1251	221	9	with	with	ADP
eurjchem-1251	221	10	water	water	NOUN
eurjchem-1251	221	11	,	,	PUNCT
eurjchem-1251	221	12	dried	dry	VERB
eurjchem-1251	221	13	and	and	CCONJ
eurjchem-1251	221	14	recrystallized	recrystallize	VERB
eurjchem-1251	221	15	from	from	ADP
eurjchem-1251	221	16	ethanol	ethanol	NOUN
eurjchem-1251	221	17	(	(	PUNCT
eurjchem-1251	221	18	scheme	scheme	NOUN
eurjchem-1251	221	19	3	3	NUM
eurjchem-1251	221	20	)	)	PUNCT
eurjchem-1251	221	21	.	.	PUNCT
eurjchem-1251	222	1	color	color	NOUN
eurjchem-1251	222	2	:	:	PUNCT
eurjchem-1251	222	3	dark	dark	PROPN
eurjchem-1251	222	4	brown	brown	PROPN
eurjchem-1251	222	5	.	.	PUNCT
eurjchem-1251	223	1	yield	yield	NOUN
eurjchem-1251	223	2	:	:	PUNCT
eurjchem-1251	223	3	81.20	81.20	NUM
eurjchem-1251	223	4	%	%	NOUN
eurjchem-1251	223	5	.	.	PUNCT
eurjchem-1251	224	1	m.p	m.p	PROPN
eurjchem-1251	224	2	.	.	PROPN
eurjchem-1251	224	3	:	:	PUNCT
eurjchem-1251	225	1	>	>	X
eurjchem-1251	225	2	300	300	NUM
eurjchem-1251	225	3	°	°	SYM
eurjchem-1251	225	4	c	c	NOUN
eurjchem-1251	225	5	.	.	PUNCT
eurjchem-1251	226	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	226	2	(	(	PUNCT
eurjchem-1251	226	3	kbr	kbr	PROPN
eurjchem-1251	226	4	,	,	PUNCT
eurjchem-1251	226	5	ν	ν	PROPN
eurjchem-1251	226	6	,	,	PUNCT
eurjchem-1251	226	7	cm‐1	cm‐1	PROPN
eurjchem-1251	226	8	):	):	PUNCT
eurjchem-1251	226	9	3384	3384	NUM
eurjchem-1251	226	10	(	(	PUNCT
eurjchem-1251	226	11	oh	oh	INTJ
eurjchem-1251	226	12	acid	acid	NOUN
eurjchem-1251	226	13	)	)	PUNCT
eurjchem-1251	226	14	,	,	PUNCT
eurjchem-1251	226	15	3059	3059	NUM
eurjchem-1251	226	16	(	(	PUNCT
eurjchem-1251	226	17	ch	ch	NOUN
eurjchem-1251	226	18	arom	arom	NOUN
eurjchem-1251	226	19	.	.	PUNCT
eurjchem-1251	226	20	)	)	PUNCT
eurjchem-1251	226	21	,	,	PUNCT
eurjchem-1251	226	22	2922	2922	NUM
eurjchem-1251	226	23	,	,	PUNCT
eurjchem-1251	226	24	2852	2852	NUM
eurjchem-1251	226	25	(	(	PUNCT
eurjchem-1251	226	26	ch	ch	NOUN
eurjchem-1251	226	27	aliph	aliph	PROPN
eurjchem-1251	226	28	.	.	PUNCT
eurjchem-1251	226	29	)	)	PUNCT
eurjchem-1251	226	30	,	,	PUNCT
eurjchem-1251	226	31	1714	1714	NUM
eurjchem-1251	226	32	(	(	PUNCT
eurjchem-1251	226	33	c	c	NOUN
eurjchem-1251	226	34	=	=	NOUN
eurjchem-1251	226	35	o	o	NOUN
eurjchem-1251	226	36	acid	acid	NOUN
eurjchem-1251	226	37	)	)	PUNCT
eurjchem-1251	226	38	.	.	PUNCT
eurjchem-1251	227	1	1h	1h	NUM
eurjchem-1251	227	2	nmr	nmr	NOUN
eurjchem-1251	227	3	(	(	PUNCT
eurjchem-1251	227	4	300	300	NUM
eurjchem-1251	227	5	mhz	mhz	NOUN
eurjchem-1251	227	6	,	,	PUNCT
eurjchem-1251	227	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	227	8	,	,	PUNCT
eurjchem-1251	227	9	δ	δ	PROPN
eurjchem-1251	227	10	,	,	PUNCT
eurjchem-1251	227	11	ppm	ppm	NOUN
eurjchem-1251	227	12	):	):	PUNCT
eurjchem-1251	227	13	1.95	1.95	NUM
eurjchem-1251	227	14	(	(	PUNCT
eurjchem-1251	227	15	s	s	PROPN
eurjchem-1251	227	16	,	,	PUNCT
eurjchem-1251	227	17	3h	3h	NUM
eurjchem-1251	227	18	,	,	PUNCT
eurjchem-1251	227	19	ch3	ch3	PROPN
eurjchem-1251	227	20	)	)	PUNCT
eurjchem-1251	227	21	,	,	PUNCT
eurjchem-1251	227	22	2.71(s	2.71(s	NUM
eurjchem-1251	227	23	,	,	PUNCT
eurjchem-1251	227	24	2h	2h	NUM
eurjchem-1251	227	25	,	,	PUNCT
eurjchem-1251	227	26	ch2	ch2	PROPN
eurjchem-1251	227	27	)	)	PUNCT
eurjchem-1251	227	28	,	,	PUNCT
eurjchem-1251	227	29	7.41‐7.79	7.41‐7.79	X
eurjchem-1251	227	30	(	(	PUNCT
eurjchem-1251	227	31	m	m	PROPN
eurjchem-1251	227	32	,	,	PUNCT
eurjchem-1251	227	33	15h	15h	NUM
eurjchem-1251	227	34	,	,	PUNCT
eurjchem-1251	227	35	3ph	3ph	NOUN
eurjchem-1251	227	36	)	)	PUNCT
eurjchem-1251	227	37	11.03	11.03	NUM
eurjchem-1251	227	38	(	(	PUNCT
eurjchem-1251	227	39	s	s	PROPN
eurjchem-1251	227	40	,	,	PUNCT
eurjchem-1251	227	41	1h	1h	NUM
eurjchem-1251	227	42	,	,	PUNCT
eurjchem-1251	227	43	cooh	cooh	NOUN
eurjchem-1251	227	44	)	)	PUNCT
eurjchem-1251	227	45	.	.	PUNCT
eurjchem-1251	228	1	ms	ms	NOUN
eurjchem-1251	228	2	(	(	PUNCT
eurjchem-1251	228	3	ei	ei	PROPN
eurjchem-1251	228	4	,	,	PUNCT
eurjchem-1251	228	5	m	m	PROPN
eurjchem-1251	228	6	/	/	SYM
eurjchem-1251	228	7	z	z	PROPN
eurjchem-1251	228	8	(	(	PUNCT
eurjchem-1251	228	9	%	%	NOUN
eurjchem-1251	228	10	)	)	PUNCT
eurjchem-1251	228	11	):	):	PUNCT
eurjchem-1251	228	12	407	407	NUM
eurjchem-1251	228	13	(	(	PUNCT
eurjchem-1251	228	14	m+	m+	NUM
eurjchem-1251	228	15	,	,	PUNCT
eurjchem-1251	228	16	38.30	38.30	NUM
eurjchem-1251	228	17	)	)	PUNCT
eurjchem-1251	228	18	,	,	PUNCT
eurjchem-1251	228	19	392	392	NUM
eurjchem-1251	228	20	(	(	PUNCT
eurjchem-1251	228	21	39.01	39.01	NUM
eurjchem-1251	228	22	)	)	PUNCT
eurjchem-1251	228	23	,	,	PUNCT
eurjchem-1251	228	24	379	379	NUM
eurjchem-1251	228	25	(	(	PUNCT
eurjchem-1251	228	26	41.13	41.13	NUM
eurjchem-1251	228	27	)	)	PUNCT
eurjchem-1251	228	28	,	,	PUNCT
eurjchem-1251	228	29	361	361	NUM
eurjchem-1251	228	30	(	(	PUNCT
eurjchem-1251	228	31	43.97	43.97	NUM
eurjchem-1251	228	32	)	)	PUNCT
eurjchem-1251	228	33	,	,	PUNCT
eurjchem-1251	228	34	348	348	NUM
eurjchem-1251	228	35	(	(	PUNCT
eurjchem-1251	228	36	48.23	48.23	NUM
eurjchem-1251	228	37	)	)	PUNCT
eurjchem-1251	228	38	,	,	PUNCT
eurjchem-1251	228	39	307	307	NUM
eurjchem-1251	228	40	(	(	PUNCT
eurjchem-1251	228	41	46.10	46.10	NUM
eurjchem-1251	228	42	)	)	PUNCT
eurjchem-1251	228	43	,	,	PUNCT
eurjchem-1251	228	44	303	303	NUM
eurjchem-1251	228	45	(	(	PUNCT
eurjchem-1251	228	46	40.43	40.43	NUM
eurjchem-1251	228	47	)	)	PUNCT
eurjchem-1251	228	48	,	,	PUNCT
eurjchem-1251	228	49	267	267	NUM
eurjchem-1251	228	50	(	(	PUNCT
eurjchem-1251	228	51	44.68	44.68	NUM
eurjchem-1251	228	52	)	)	PUNCT
eurjchem-1251	228	53	,	,	PUNCT
eurjchem-1251	228	54	141	141	NUM
eurjchem-1251	228	55	(	(	PUNCT
eurjchem-1251	228	56	52.48	52.48	NUM
eurjchem-1251	228	57	)	)	PUNCT
eurjchem-1251	228	58	,	,	PUNCT
eurjchem-1251	228	59	104	104	NUM
eurjchem-1251	228	60	(	(	PUNCT
eurjchem-1251	228	61	11.35	11.35	NUM
eurjchem-1251	228	62	)	)	PUNCT
eurjchem-1251	228	63	,	,	PUNCT
eurjchem-1251	228	64	100	100	NUM
eurjchem-1251	228	65	(	(	PUNCT
eurjchem-1251	228	66	42.55	42.55	NUM
eurjchem-1251	228	67	)	)	PUNCT
eurjchem-1251	228	68	,	,	PUNCT
eurjchem-1251	228	69	58	58	NUM
eurjchem-1251	228	70	(	(	PUNCT
eurjchem-1251	228	71	8.51	8.51	NUM
eurjchem-1251	228	72	)	)	PUNCT
eurjchem-1251	228	73	,	,	PUNCT
eurjchem-1251	228	74	57	57	NUM
eurjchem-1251	228	75	(	(	PUNCT
eurjchem-1251	228	76	100	100	NUM
eurjchem-1251	228	77	)	)	PUNCT
eurjchem-1251	228	78	.	.	PUNCT
eurjchem-1251	229	1	anal	anal	PROPN
eurjchem-1251	229	2	.	.	PUNCT
eurjchem-1251	229	3	calcd	calcd	NOUN
eurjchem-1251	229	4	.	.	PUNCT
eurjchem-1251	230	1	for	for	ADP
eurjchem-1251	230	2	c26h21n3o2	c26h21n3o2	PROPN
eurjchem-1251	230	3	:	:	PUNCT
eurjchem-1251	230	4	c	c	X
eurjchem-1251	230	5	,	,	PUNCT
eurjchem-1251	230	6	76.64	76.64	NUM
eurjchem-1251	230	7	;	;	PUNCT
eurjchem-1251	230	8	h	h	NOUN
eurjchem-1251	230	9	,	,	PUNCT
eurjchem-1251	230	10	5.19	5.19	NUM
eurjchem-1251	230	11	;	;	PUNCT
eurjchem-1251	230	12	n	n	CCONJ
eurjchem-1251	230	13	,	,	PUNCT
eurjchem-1251	230	14	10.31.found	10.31.found	NUM
eurjchem-1251	230	15	:	:	PUNCT
eurjchem-1251	230	16	c	c	X
eurjchem-1251	230	17	,	,	PUNCT
eurjchem-1251	230	18	76.90	76.90	NUM
eurjchem-1251	230	19	;	;	PUNCT
eurjchem-1251	230	20	h	h	NOUN
eurjchem-1251	230	21	,	,	PUNCT
eurjchem-1251	230	22	5.40	5.40	NUM
eurjchem-1251	230	23	;	;	PUNCT
eurjchem-1251	230	24	n	n	CCONJ
eurjchem-1251	230	25	,	,	PUNCT
eurjchem-1251	230	26	10.50	10.50	NUM
eurjchem-1251	230	27	%	%	NOUN
eurjchem-1251	230	28	.	.	PUNCT
eurjchem-1251	231	1	2.2.19	2.2.19	NUM
eurjchem-1251	231	2	.	.	PUNCT
eurjchem-1251	232	1	synthesis	synthesis	NOUN
eurjchem-1251	232	2	of	of	ADP
eurjchem-1251	232	3	n‐(4,5,6‐triphenylpyridazin‐3‐yl	n‐(4,5,6‐triphenylpyridazin‐3‐yl	NOUN
eurjchem-1251	232	4	)	)	PUNCT
eurjchem-1251	232	5	benzoylacetamide	benzoylacetamide	NOUN
eurjchem-1251	232	6	(	(	PUNCT
eurjchem-1251	232	7	13	13	NUM
eurjchem-1251	232	8	)	)	PUNCT
eurjchem-1251	232	9	a	a	DET
eurjchem-1251	232	10	mixture	mixture	NOUN
eurjchem-1251	232	11	of	of	ADP
eurjchem-1251	232	12	compound	compound	NOUN
eurjchem-1251	232	13	5	5	NUM
eurjchem-1251	232	14	(	(	PUNCT
eurjchem-1251	232	15	0.5	0.5	NUM
eurjchem-1251	232	16	g	g	NOUN
eurjchem-1251	232	17	,	,	PUNCT
eurjchem-1251	232	18	1.55	1.55	NUM
eurjchem-1251	232	19	mmol	mmol	NOUN
eurjchem-1251	232	20	)	)	PUNCT
eurjchem-1251	232	21	and	and	CCONJ
eurjchem-1251	232	22	ethyl	ethyl	PROPN
eurjchem-1251	232	23	benzoylacetate	benzoylacetate	NOUN
eurjchem-1251	232	24	(	(	PUNCT
eurjchem-1251	232	25	0.27	0.27	NUM
eurjchem-1251	232	26	ml	ml	NOUN
eurjchem-1251	232	27	,	,	PUNCT
eurjchem-1251	232	28	1.55	1.55	NUM
eurjchem-1251	232	29	mmol	mmol	NOUN
eurjchem-1251	232	30	)	)	PUNCT
eurjchem-1251	232	31	was	be	AUX
eurjchem-1251	232	32	heated	heat	VERB
eurjchem-1251	232	33	under	under	ADP
eurjchem-1251	232	34	reflux	reflux	NOUN
eurjchem-1251	232	35	for	for	ADP
eurjchem-1251	232	36	1	1	NUM
eurjchem-1251	232	37	h.	h.	NOUN
eurjchem-1251	232	38	after	after	ADP
eurjchem-1251	232	39	cooling	cool	VERB
eurjchem-1251	232	40	,	,	PUNCT
eurjchem-1251	232	41	the	the	DET
eurjchem-1251	232	42	reaction	reaction	NOUN
eurjchem-1251	232	43	mixture	mixture	NOUN
eurjchem-1251	232	44	was	be	AUX
eurjchem-1251	232	45	treated	treat	VERB
eurjchem-1251	232	46	with	with	ADP
eurjchem-1251	232	47	diethyl	diethyl	NOUN
eurjchem-1251	232	48	ether	ether	NOUN
eurjchem-1251	232	49	(	(	PUNCT
eurjchem-1251	232	50	50	50	NUM
eurjchem-1251	232	51	ml	ml	NOUN
eurjchem-1251	232	52	)	)	PUNCT
eurjchem-1251	232	53	,	,	PUNCT
eurjchem-1251	232	54	and	and	CCONJ
eurjchem-1251	232	55	the	the	DET
eurjchem-1251	232	56	solid	solid	ADJ
eurjchem-1251	232	57	product	product	NOUN
eurjchem-1251	232	58	was	be	AUX
eurjchem-1251	232	59	filtered	filter	VERB
eurjchem-1251	232	60	off	off	ADP
eurjchem-1251	232	61	,	,	PUNCT
eurjchem-1251	232	62	dried	dry	VERB
eurjchem-1251	232	63	and	and	CCONJ
eurjchem-1251	232	64	recrystallized	recrystallize	VERB
eurjchem-1251	232	65	from	from	ADP
eurjchem-1251	232	66	ethanol	ethanol	NOUN
eurjchem-1251	232	67	(	(	PUNCT
eurjchem-1251	232	68	scheme	scheme	NOUN
eurjchem-1251	232	69	3	3	NUM
eurjchem-1251	232	70	)	)	PUNCT
eurjchem-1251	232	71	.	.	PUNCT
eurjchem-1251	233	1	color	color	NOUN
eurjchem-1251	233	2	:	:	PUNCT
eurjchem-1251	233	3	dark	dark	PROPN
eurjchem-1251	233	4	brown	brown	PROPN
eurjchem-1251	233	5	.	.	PUNCT
eurjchem-1251	234	1	yield	yield	NOUN
eurjchem-1251	234	2	:	:	PUNCT
eurjchem-1251	234	3	68.87	68.87	NUM
eurjchem-1251	234	4	%	%	NOUN
eurjchem-1251	234	5	.	.	PUNCT
eurjchem-1251	235	1	m.p	m.p	PROPN
eurjchem-1251	235	2	.	.	PROPN
eurjchem-1251	235	3	:	:	PUNCT
eurjchem-1251	236	1	190‐192	190‐192	NUM
eurjchem-1251	236	2	°	°	ADP
eurjchem-1251	236	3	c	c	X
eurjchem-1251	236	4	.	.	PUNCT
eurjchem-1251	237	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	237	2	(	(	PUNCT
eurjchem-1251	237	3	kbr	kbr	PROPN
eurjchem-1251	237	4	,	,	PUNCT
eurjchem-1251	237	5	ν	ν	PROPN
eurjchem-1251	237	6	,	,	PUNCT
eurjchem-1251	237	7	cm‐1	cm‐1	PROPN
eurjchem-1251	237	8	):	):	PUNCT
eurjchem-1251	237	9	3429	3429	NUM
eurjchem-1251	237	10	(	(	PUNCT
eurjchem-1251	237	11	nh	nh	NOUN
eurjchem-1251	237	12	amide	amide	NOUN
eurjchem-1251	237	13	)	)	PUNCT
eurjchem-1251	237	14	,	,	PUNCT
eurjchem-1251	237	15	3058	3058	NUM
eurjchem-1251	237	16	(	(	PUNCT
eurjchem-1251	237	17	ch	ch	NOUN
eurjchem-1251	237	18	arom	arom	NOUN
eurjchem-1251	237	19	.	.	PUNCT
eurjchem-1251	237	20	)	)	PUNCT
eurjchem-1251	237	21	,	,	PUNCT
eurjchem-1251	237	22	2925	2925	NUM
eurjchem-1251	237	23	(	(	PUNCT
eurjchem-1251	237	24	ch	ch	NOUN
eurjchem-1251	237	25	aliph	aliph	PROPN
eurjchem-1251	237	26	.	.	PUNCT
eurjchem-1251	237	27	)	)	PUNCT
eurjchem-1251	237	28	,	,	PUNCT
eurjchem-1251	237	29	1723	1723	NUM
eurjchem-1251	237	30	(	(	PUNCT
eurjchem-1251	237	31	c	c	NOUN
eurjchem-1251	237	32	=	=	NOUN
eurjchem-1251	237	33	o	o	X
eurjchem-1251	237	34	ketone	ketone	NOUN
eurjchem-1251	237	35	)	)	PUNCT
eurjchem-1251	237	36	,	,	PUNCT
eurjchem-1251	237	37	1677	1677	NUM
eurjchem-1251	237	38	(	(	PUNCT
eurjchem-1251	237	39	c	c	NOUN
eurjchem-1251	237	40	=	=	SYM
eurjchem-1251	237	41	o	o	NOUN
eurjchem-1251	237	42	,	,	PUNCT
eurjchem-1251	237	43	amide	amide	NOUN
eurjchem-1251	237	44	)	)	PUNCT
eurjchem-1251	237	45	.	.	PUNCT
eurjchem-1251	238	1	1h	1h	NUM
eurjchem-1251	238	2	nmr	nmr	NOUN
eurjchem-1251	238	3	(	(	PUNCT
eurjchem-1251	238	4	300	300	NUM
eurjchem-1251	238	5	mhz	mhz	NOUN
eurjchem-1251	238	6	,	,	PUNCT
eurjchem-1251	238	7	dmso‐	dmso‐	NUM
eurjchem-1251	238	8	d6	d6	NOUN
eurjchem-1251	238	9	,	,	PUNCT
eurjchem-1251	238	10	δ	δ	PROPN
eurjchem-1251	238	11	,	,	PUNCT
eurjchem-1251	238	12	ppm	ppm	NUM
eurjchem-1251	238	13	):	):	PUNCT
eurjchem-1251	238	14	3.31	3.31	NUM
eurjchem-1251	238	15	(	(	PUNCT
eurjchem-1251	238	16	s	s	PROPN
eurjchem-1251	238	17	,	,	PUNCT
eurjchem-1251	238	18	2h	2h	NUM
eurjchem-1251	238	19	,	,	PUNCT
eurjchem-1251	238	20	ch2	ch2	PROPN
eurjchem-1251	238	21	)	)	PUNCT
eurjchem-1251	238	22	,	,	PUNCT
eurjchem-1251	238	23	7.11‐7.82	7.11‐7.82	PROPN
eurjchem-1251	238	24	(	(	PUNCT
eurjchem-1251	238	25	m	m	PROPN
eurjchem-1251	238	26	,	,	PUNCT
eurjchem-1251	238	27	20h	20h	NOUN
eurjchem-1251	238	28	,	,	PUNCT
eurjchem-1251	238	29	4ph	4ph	NOUN
eurjchem-1251	238	30	)	)	PUNCT
eurjchem-1251	238	31	,	,	PUNCT
eurjchem-1251	238	32	7.97	7.97	NUM
eurjchem-1251	238	33	(	(	PUNCT
eurjchem-1251	238	34	s	s	PROPN
eurjchem-1251	238	35	,	,	PUNCT
eurjchem-1251	238	36	1h	1h	NUM
eurjchem-1251	238	37	,	,	PUNCT
eurjchem-1251	238	38	nh	nh	PROPN
eurjchem-1251	238	39	)	)	PUNCT
eurjchem-1251	238	40	.	.	PUNCT
eurjchem-1251	239	1	ms	ms	NOUN
eurjchem-1251	239	2	(	(	PUNCT
eurjchem-1251	239	3	ei	ei	PROPN
eurjchem-1251	239	4	,	,	PUNCT
eurjchem-1251	239	5	m	m	PROPN
eurjchem-1251	239	6	/	/	SYM
eurjchem-1251	239	7	z	z	PROPN
eurjchem-1251	239	8	(	(	PUNCT
eurjchem-1251	239	9	%	%	NOUN
eurjchem-1251	239	10	)	)	PUNCT
eurjchem-1251	239	11	):	):	PUNCT
eurjchem-1251	239	12	469	469	NUM
eurjchem-1251	239	13	(	(	PUNCT
eurjchem-1251	239	14	m+	m+	NUM
eurjchem-1251	239	15	,	,	PUNCT
eurjchem-1251	239	16	4.09	4.09	NUM
eurjchem-1251	239	17	)	)	PUNCT
eurjchem-1251	239	18	,	,	PUNCT
eurjchem-1251	239	19	363	363	NUM
eurjchem-1251	239	20	(	(	PUNCT
eurjchem-1251	239	21	3.21	3.21	NUM
eurjchem-1251	239	22	)	)	PUNCT
eurjchem-1251	239	23	,	,	PUNCT
eurjchem-1251	239	24	350	350	NUM
eurjchem-1251	239	25	(	(	PUNCT
eurjchem-1251	239	26	4.94	4.94	NUM
eurjchem-1251	239	27	)	)	PUNCT
eurjchem-1251	239	28	,	,	PUNCT
eurjchem-1251	239	29	322	322	NUM
eurjchem-1251	239	30	(	(	PUNCT
eurjchem-1251	239	31	5.34	5.34	NUM
eurjchem-1251	239	32	)	)	PUNCT
eurjchem-1251	239	33	,	,	PUNCT
eurjchem-1251	239	34	291	291	NUM
eurjchem-1251	239	35	(	(	PUNCT
eurjchem-1251	239	36	11.45	11.45	NUM
eurjchem-1251	239	37	)	)	PUNCT
eurjchem-1251	239	38	,	,	PUNCT
eurjchem-1251	239	39	263	263	NUM
eurjchem-1251	239	40	(	(	PUNCT
eurjchem-1251	239	41	5.51	5.51	NUM
eurjchem-1251	239	42	)	)	PUNCT
eurjchem-1251	239	43	,	,	PUNCT
eurjchem-1251	239	44	206	206	NUM
eurjchem-1251	239	45	(	(	PUNCT
eurjchem-1251	239	46	4.12	4.12	NUM
eurjchem-1251	239	47	)	)	PUNCT
eurjchem-1251	239	48	,	,	PUNCT
eurjchem-1251	239	49	177	177	NUM
eurjchem-1251	239	50	(	(	PUNCT
eurjchem-1251	239	51	5.60	5.60	NUM
eurjchem-1251	239	52	)	)	PUNCT
eurjchem-1251	239	53	,	,	PUNCT
eurjchem-1251	239	54	163	163	NUM
eurjchem-1251	239	55	(	(	PUNCT
eurjchem-1251	239	56	4.32	4.32	NUM
eurjchem-1251	239	57	)	)	PUNCT
eurjchem-1251	239	58	,	,	PUNCT
eurjchem-1251	239	59	105	105	NUM
eurjchem-1251	239	60	(	(	PUNCT
eurjchem-1251	239	61	89.44	89.44	NUM
eurjchem-1251	239	62	)	)	PUNCT
eurjchem-1251	239	63	,	,	PUNCT
eurjchem-1251	239	64	103	103	NUM
eurjchem-1251	239	65	(	(	PUNCT
eurjchem-1251	239	66	7.46	7.46	NUM
eurjchem-1251	239	67	)	)	PUNCT
eurjchem-1251	239	68	,	,	PUNCT
eurjchem-1251	239	69	77	77	NUM
eurjchem-1251	239	70	(	(	PUNCT
eurjchem-1251	239	71	100	100	NUM
eurjchem-1251	239	72	)	)	PUNCT
eurjchem-1251	239	73	.	.	PUNCT
eurjchem-1251	240	1	anal	anal	PROPN
eurjchem-1251	240	2	.	.	PUNCT
eurjchem-1251	240	3	calcd	calcd	NOUN
eurjchem-1251	240	4	.	.	PUNCT
eurjchem-1251	241	1	for	for	ADP
eurjchem-1251	241	2	c31h23n3o2	c31h23n3o2	PROPN
eurjchem-1251	241	3	:	:	PUNCT
eurjchem-1251	241	4	c	c	X
eurjchem-1251	241	5	,	,	PUNCT
eurjchem-1251	241	6	79.30	79.30	NUM
eurjchem-1251	241	7	;	;	PUNCT
eurjchem-1251	241	8	h	h	NOUN
eurjchem-1251	241	9	,	,	PUNCT
eurjchem-1251	241	10	4.94	4.94	NUM
eurjchem-1251	241	11	;	;	PUNCT
eurjchem-1251	241	12	n	n	CCONJ
eurjchem-1251	241	13	,	,	PUNCT
eurjchem-1251	241	14	8.95	8.95	NUM
eurjchem-1251	241	15	.	.	PUNCT
eurjchem-1251	241	16	found	find	VERB
eurjchem-1251	241	17	:	:	PUNCT
eurjchem-1251	242	1	c	c	X
eurjchem-1251	242	2	,	,	PUNCT
eurjchem-1251	242	3	79.60	79.60	NUM
eurjchem-1251	242	4	;	;	PUNCT
eurjchem-1251	242	5	h	h	NOUN
eurjchem-1251	242	6	,	,	PUNCT
eurjchem-1251	242	7	5.10	5.10	NUM
eurjchem-1251	242	8	;	;	PUNCT
eurjchem-1251	242	9	n	n	CCONJ
eurjchem-1251	242	10	,	,	PUNCT
eurjchem-1251	242	11	8.50	8.50	NUM
eurjchem-1251	242	12	%	%	NOUN
eurjchem-1251	242	13	.	.	PUNCT
eurjchem-1251	243	1	2.2.20	2.2.20	NUM
eurjchem-1251	243	2	.	.	PUNCT
eurjchem-1251	243	3	general	general	ADJ
eurjchem-1251	243	4	procedure	procedure	NOUN
eurjchem-1251	243	5	for	for	ADP
eurjchem-1251	243	6	the	the	DET
eurjchem-1251	243	7	reaction	reaction	NOUN
eurjchem-1251	243	8	of	of	ADP
eurjchem-1251	243	9	3‐chloro‐4,5,6‐	3‐chloro‐4,5,6‐	NUM
eurjchem-1251	243	10	triphenylpyridazine	triphenylpyridazine	NOUN
eurjchem-1251	243	11	(	(	PUNCT
eurjchem-1251	243	12	2	2	NUM
eurjchem-1251	243	13	)	)	PUNCT
eurjchem-1251	243	14	with	with	ADP
eurjchem-1251	243	15	4‐aminobenzenesulfonamide	4‐aminobenzenesulfonamide	NUM
eurjchem-1251	243	16	derivatives	derivative	NOUN
eurjchem-1251	243	17	(	(	PUNCT
eurjchem-1251	243	18	14a‐g	14a‐g	NUM
eurjchem-1251	243	19	)	)	PUNCT
eurjchem-1251	243	20	a	a	DET
eurjchem-1251	243	21	mixture	mixture	NOUN
eurjchem-1251	243	22	of	of	ADP
eurjchem-1251	243	23	compound	compound	NOUN
eurjchem-1251	243	24	2	2	NUM
eurjchem-1251	243	25	(	(	PUNCT
eurjchem-1251	243	26	0.5	0.5	NUM
eurjchem-1251	243	27	g	g	NOUN
eurjchem-1251	243	28	,	,	PUNCT
eurjchem-1251	243	29	1.46	1.46	NUM
eurjchem-1251	243	30	mmol	mmol	NOUN
eurjchem-1251	243	31	)	)	PUNCT
eurjchem-1251	243	32	and	and	CCONJ
eurjchem-1251	243	33	4‐	4‐	NUM
eurjchem-1251	243	34	aminobenzenesulfonamide	aminobenzenesulfonamide	VERB
eurjchem-1251	243	35	derivatives	derivative	NOUN
eurjchem-1251	243	36	14a‐g	14a‐g	NOUN
eurjchem-1251	243	37	(	(	PUNCT
eurjchem-1251	243	38	1.46	1.46	NUM
eurjchem-1251	243	39	mmol	mmol	NOUN
eurjchem-1251	243	40	)	)	PUNCT
eurjchem-1251	243	41	in	in	ADP
eurjchem-1251	243	42	n‐butanol	n‐butanol	PROPN
eurjchem-1251	243	43	(	(	PUNCT
eurjchem-1251	243	44	10	10	NUM
eurjchem-1251	243	45	ml	ml	NOUN
eurjchem-1251	243	46	)	)	PUNCT
eurjchem-1251	243	47	was	be	AUX
eurjchem-1251	243	48	refluxed	refluxe	VERB
eurjchem-1251	243	49	for	for	ADP
eurjchem-1251	243	50	5	5	NUM
eurjchem-1251	243	51	h	h	NOUN
eurjchem-1251	243	52	,	,	PUNCT
eurjchem-1251	243	53	cooled	cool	VERB
eurjchem-1251	243	54	to	to	ADP
eurjchem-1251	243	55	room	room	NOUN
eurjchem-1251	243	56	temperature	temperature	NOUN
eurjchem-1251	243	57	,	,	PUNCT
eurjchem-1251	243	58	and	and	CCONJ
eurjchem-1251	243	59	the	the	DET
eurjchem-1251	243	60	separated	separate	VERB
eurjchem-1251	243	61	solid	solid	ADJ
eurjchem-1251	243	62	was	be	AUX
eurjchem-1251	243	63	filtered	filter	VERB
eurjchem-1251	243	64	off	off	ADP
eurjchem-1251	243	65	,	,	PUNCT
eurjchem-1251	243	66	washed	wash	VERB
eurjchem-1251	243	67	with	with	ADP
eurjchem-1251	243	68	water	water	NOUN
eurjchem-1251	243	69	,	,	PUNCT
eurjchem-1251	243	70	dried	dry	VERB
eurjchem-1251	243	71	,	,	PUNCT
eurjchem-1251	243	72	and	and	CCONJ
eurjchem-1251	243	73	recrystallised	recrystallise	VERB
eurjchem-1251	243	74	from	from	ADP
eurjchem-1251	243	75	ethanol	ethanol	NOUN
eurjchem-1251	243	76	to	to	ADP
eurjchem-1251	243	77	givecompounds	givecompound	NOUN
eurjchem-1251	243	78	15a‐g	15a‐g	NOUN
eurjchem-1251	243	79	(	(	PUNCT
eurjchem-1251	243	80	scheme	scheme	NOUN
eurjchem-1251	243	81	4	4	NUM
eurjchem-1251	243	82	)	)	PUNCT
eurjchem-1251	243	83	.	.	PUNCT
eurjchem-1251	244	1	4‐[(4	4‐[(4	NUM
eurjchem-1251	244	2	,	,	PUNCT
eurjchem-1251	244	3	5	5	NUM
eurjchem-1251	244	4	,	,	PUNCT
eurjchem-1251	244	5	6‐triphenylpyridazin‐3‐yl)amino]benzenesulfon	6‐triphenylpyridazin‐3‐yl)amino]benzenesulfon	NUM
eurjchem-1251	244	6	amide	amide	NOUN
eurjchem-1251	244	7	(	(	PUNCT
eurjchem-1251	244	8	15a	15a	NOUN
eurjchem-1251	244	9	):	):	PUNCT
eurjchem-1251	244	10	color	color	NOUN
eurjchem-1251	244	11	:	:	PUNCT
eurjchem-1251	244	12	white	white	ADJ
eurjchem-1251	244	13	.	.	PUNCT
eurjchem-1251	245	1	yield	yield	NOUN
eurjchem-1251	245	2	:	:	PUNCT
eurjchem-1251	245	3	81.66	81.66	NUM
eurjchem-1251	245	4	%	%	NOUN
eurjchem-1251	245	5	.	.	PUNCT
eurjchem-1251	246	1	m.p	m.p	PROPN
eurjchem-1251	246	2	.	.	PROPN
eurjchem-1251	246	3	:	:	PUNCT
eurjchem-1251	247	1	216‐218	216‐218	NUM
eurjchem-1251	247	2	°	°	SYM
eurjchem-1251	247	3	c	c	X
eurjchem-1251	247	4	.	.	PUNCT
eurjchem-1251	248	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	248	2	(	(	PUNCT
eurjchem-1251	248	3	kbr	kbr	PROPN
eurjchem-1251	248	4	,	,	PUNCT
eurjchem-1251	248	5	ν	ν	PROPN
eurjchem-1251	248	6	,	,	PUNCT
eurjchem-1251	248	7	cm‐1	cm‐1	PROPN
eurjchem-1251	248	8	):	):	PUNCT
eurjchem-1251	248	9	3369	3369	NUM
eurjchem-1251	248	10	,	,	PUNCT
eurjchem-1251	248	11	3294	3294	NUM
eurjchem-1251	248	12	,	,	PUNCT
eurjchem-1251	248	13	3214	3214	NUM
eurjchem-1251	248	14	(	(	PUNCT
eurjchem-1251	248	15	nh	nh	PROPN
eurjchem-1251	248	16	,	,	PUNCT
eurjchem-1251	248	17	nh2	nh2	PROPN
eurjchem-1251	248	18	)	)	PUNCT
eurjchem-1251	248	19	,	,	PUNCT
eurjchem-1251	248	20	3078	3078	NUM
eurjchem-1251	248	21	(	(	PUNCT
eurjchem-1251	248	22	ch	ch	NOUN
eurjchem-1251	248	23	arom	arom	NOUN
eurjchem-1251	248	24	.	.	PUNCT
eurjchem-1251	248	25	)	)	PUNCT
eurjchem-1251	248	26	,	,	PUNCT
eurjchem-1251	248	27	1328	1328	NUM
eurjchem-1251	248	28	(	(	PUNCT
eurjchem-1251	248	29	so2	so2	PROPN
eurjchem-1251	248	30	asym	asym	PROPN
eurjchem-1251	248	31	.	.	PROPN
eurjchem-1251	248	32	)	)	PUNCT
eurjchem-1251	248	33	,	,	PUNCT
eurjchem-1251	248	34	1156	1156	NUM
eurjchem-1251	248	35	(	(	PUNCT
eurjchem-1251	248	36	so2	so2	PROPN
eurjchem-1251	248	37	sym	sym	PROPN
eurjchem-1251	248	38	.	.	PUNCT
eurjchem-1251	248	39	)	)	PUNCT
eurjchem-1251	248	40	.	.	PUNCT
eurjchem-1251	249	1	1h	1h	NUM
eurjchem-1251	249	2	nmr	nmr	NOUN
eurjchem-1251	249	3	(	(	PUNCT
eurjchem-1251	249	4	300	300	NUM
eurjchem-1251	249	5	mhz	mhz	NOUN
eurjchem-1251	249	6	,	,	PUNCT
eurjchem-1251	249	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	249	8	,	,	PUNCT
eurjchem-1251	249	9	δ	δ	PROPN
eurjchem-1251	249	10	,	,	PUNCT
eurjchem-1251	249	11	ppm	ppm	NOUN
eurjchem-1251	249	12	):	):	PUNCT
eurjchem-1251	249	13	7.21	7.21	NUM
eurjchem-1251	249	14	(	(	PUNCT
eurjchem-1251	249	15	s	s	PROPN
eurjchem-1251	249	16	,	,	PUNCT
eurjchem-1251	249	17	2h	2h	NUM
eurjchem-1251	249	18	,	,	PUNCT
eurjchem-1251	249	19	nh2	nh2	PROPN
eurjchem-1251	249	20	)	)	PUNCT
eurjchem-1251	249	21	,	,	PUNCT
eurjchem-1251	249	22	7.70‐7.76	7.70‐7.76	NUM
eurjchem-1251	249	23	(	(	PUNCT
eurjchem-1251	249	24	m	m	PROPN
eurjchem-1251	249	25	,	,	PUNCT
eurjchem-1251	249	26	19h	19h	X
eurjchem-1251	249	27	,	,	PUNCT
eurjchem-1251	249	28	ar‐h	ar‐h	PROPN
eurjchem-1251	249	29	)	)	PUNCT
eurjchem-1251	249	30	,	,	PUNCT
eurjchem-1251	249	31	10.25	10.25	NUM
eurjchem-1251	249	32	(	(	PUNCT
eurjchem-1251	249	33	s	s	PROPN
eurjchem-1251	249	34	,	,	PUNCT
eurjchem-1251	249	35	1h	1h	NUM
eurjchem-1251	249	36	,	,	PUNCT
eurjchem-1251	249	37	nh	nh	PROPN
eurjchem-1251	249	38	)	)	PUNCT
eurjchem-1251	249	39	.	.	PUNCT
eurjchem-1251	250	1	ms	ms	NOUN
eurjchem-1251	250	2	(	(	PUNCT
eurjchem-1251	250	3	ei	ei	PROPN
eurjchem-1251	250	4	,	,	PUNCT
eurjchem-1251	250	5	m	m	PROPN
eurjchem-1251	250	6	/	/	SYM
eurjchem-1251	250	7	z	z	PROPN
eurjchem-1251	250	8	(	(	PUNCT
eurjchem-1251	250	9	%	%	NOUN
eurjchem-1251	250	10	)	)	PUNCT
eurjchem-1251	250	11	):	):	PUNCT
eurjchem-1251	250	12	478	478	NUM
eurjchem-1251	250	13	(	(	PUNCT
eurjchem-1251	250	14	m+	m+	NUM
eurjchem-1251	250	15	,	,	PUNCT
eurjchem-1251	250	16	25.09	25.09	NUM
eurjchem-1251	250	17	)	)	PUNCT
eurjchem-1251	250	18	,	,	PUNCT
eurjchem-1251	250	19	463	463	NUM
eurjchem-1251	250	20	(	(	PUNCT
eurjchem-1251	250	21	21.91	21.91	NUM
eurjchem-1251	250	22	)	)	PUNCT
eurjchem-1251	250	23	,	,	PUNCT
eurjchem-1251	250	24	373	373	NUM
eurjchem-1251	250	25	(	(	PUNCT
eurjchem-1251	250	26	18.37	18.37	NUM
eurjchem-1251	250	27	)	)	PUNCT
eurjchem-1251	250	28	,	,	PUNCT
eurjchem-1251	250	29	361	361	NUM
eurjchem-1251	250	30	(	(	PUNCT
eurjchem-1251	250	31	18.37	18.37	NUM
eurjchem-1251	250	32	)	)	PUNCT
eurjchem-1251	250	33	,	,	PUNCT
eurjchem-1251	250	34	322	322	NUM
eurjchem-1251	250	35	(	(	PUNCT
eurjchem-1251	250	36	19.08	19.08	NUM
eurjchem-1251	250	37	)	)	PUNCT
eurjchem-1251	250	38	,	,	PUNCT
eurjchem-1251	250	39	305	305	NUM
eurjchem-1251	250	40	(	(	PUNCT
eurjchem-1251	250	41	21.20	21.20	NUM
eurjchem-1251	250	42	)	)	PUNCT
eurjchem-1251	250	43	,	,	PUNCT
eurjchem-1251	250	44	178	178	NUM
eurjchem-1251	250	45	(	(	PUNCT
eurjchem-1251	250	46	33.57	33.57	NUM
eurjchem-1251	250	47	)	)	PUNCT
eurjchem-1251	250	48	,	,	PUNCT
eurjchem-1251	250	49	172	172	NUM
eurjchem-1251	250	50	(	(	PUNCT
eurjchem-1251	250	51	100	100	NUM
eurjchem-1251	250	52	)	)	PUNCT
eurjchem-1251	250	53	,	,	PUNCT
eurjchem-1251	250	54	118	118	NUM
eurjchem-1251	250	55	(	(	PUNCT
eurjchem-1251	250	56	8.13	8.13	NUM
eurjchem-1251	250	57	)	)	PUNCT
eurjchem-1251	250	58	,	,	PUNCT
eurjchem-1251	250	59	103	103	NUM
eurjchem-1251	250	60	(	(	PUNCT
eurjchem-1251	250	61	3.89	3.89	NUM
eurjchem-1251	250	62	)	)	PUNCT
eurjchem-1251	250	63	.	.	PUNCT
eurjchem-1251	251	1	anal	anal	PROPN
eurjchem-1251	251	2	.	.	PUNCT
eurjchem-1251	251	3	calcd	calcd	NOUN
eurjchem-1251	251	4	.	.	PUNCT
eurjchem-1251	252	1	for	for	SCONJ
eurjchem-1251	252	2	c28h22n4o2s	c28h22n4o2s	NOUN
eurjchem-1251	252	3	:	:	PUNCT
eurjchem-1251	252	4	c	c	X
eurjchem-1251	252	5	,	,	PUNCT
eurjchem-1251	252	6	70.27	70.27	NUM
eurjchem-1251	252	7	;	;	PUNCT
eurjchem-1251	252	8	h	h	NOUN
eurjchem-1251	252	9	,	,	PUNCT
eurjchem-1251	252	10	4.63	4.63	NUM
eurjchem-1251	252	11	;	;	PUNCT
eurjchem-1251	252	12	n	n	CCONJ
eurjchem-1251	252	13	,	,	PUNCT
eurjchem-1251	252	14	11.71	11.71	NUM
eurjchem-1251	252	15	.	.	PUNCT
eurjchem-1251	252	16	found	find	VERB
eurjchem-1251	252	17	:	:	PUNCT
eurjchem-1251	253	1	c	c	X
eurjchem-1251	253	2	,	,	PUNCT
eurjchem-1251	253	3	70.50	70.50	NUM
eurjchem-1251	253	4	;	;	PUNCT
eurjchem-1251	253	5	h	h	NOUN
eurjchem-1251	253	6	,	,	PUNCT
eurjchem-1251	253	7	4.70	4.70	NUM
eurjchem-1251	253	8	;	;	PUNCT
eurjchem-1251	253	9	n	n	CCONJ
eurjchem-1251	253	10	,	,	PUNCT
eurjchem-1251	253	11	11.40	11.40	NUM
eurjchem-1251	253	12	%	%	NOUN
eurjchem-1251	253	13	.	.	PUNCT
eurjchem-1251	254	1	n‐benzyl‐4‐[(4	n‐benzyl‐4‐[(4	NOUN
eurjchem-1251	254	2	,	,	PUNCT
eurjchem-1251	254	3	5	5	NUM
eurjchem-1251	254	4	,	,	PUNCT
eurjchem-1251	254	5	6‐triphenylpyridazin‐3‐yl)amino]benzene	6‐triphenylpyridazin‐3‐yl)amino]benzene	NOUN
eurjchem-1251	254	6	sulfonamide	sulfonamide	NOUN
eurjchem-1251	254	7	(	(	PUNCT
eurjchem-1251	254	8	15b	15b	NUM
eurjchem-1251	254	9	):	):	PUNCT
eurjchem-1251	254	10	color	color	NOUN
eurjchem-1251	254	11	:	:	PUNCT
eurjchem-1251	254	12	white	white	ADJ
eurjchem-1251	254	13	.	.	PUNCT
eurjchem-1251	255	1	yield	yield	NOUN
eurjchem-1251	255	2	:	:	PUNCT
eurjchem-1251	255	3	90.43	90.43	NUM
eurjchem-1251	255	4	%	%	NOUN
eurjchem-1251	255	5	.	.	PUNCT
eurjchem-1251	256	1	m.p	m.p	PROPN
eurjchem-1251	256	2	.	.	PROPN
eurjchem-1251	256	3	:	:	PUNCT
eurjchem-1251	257	1	118‐120	118‐120	NUM
eurjchem-1251	258	1	°	°	PROPN
eurjchem-1251	258	2	c	c	X
eurjchem-1251	258	3	.	.	PUNCT
eurjchem-1251	258	4	ft‐ir	ft‐ir	NOUN
eurjchem-1251	258	5	(	(	PUNCT
eurjchem-1251	258	6	kbr	kbr	PROPN
eurjchem-1251	258	7	,	,	PUNCT
eurjchem-1251	258	8	ν	ν	PROPN
eurjchem-1251	258	9	,	,	PUNCT
eurjchem-1251	258	10	cm‐1	cm‐1	PROPN
eurjchem-1251	258	11	):	):	PUNCT
eurjchem-1251	258	12	3379	3379	NUM
eurjchem-1251	258	13	,	,	PUNCT
eurjchem-1251	258	14	3292	3292	NUM
eurjchem-1251	258	15	(	(	PUNCT
eurjchem-1251	258	16	2nh	2nh	NOUN
eurjchem-1251	258	17	)	)	PUNCT
eurjchem-1251	258	18	,	,	PUNCT
eurjchem-1251	258	19	3064	3064	NUM
eurjchem-1251	258	20	(	(	PUNCT
eurjchem-1251	258	21	ch	ch	NOUN
eurjchem-1251	258	22	arom	arom	NOUN
eurjchem-1251	258	23	.	.	PUNCT
eurjchem-1251	258	24	)	)	PUNCT
eurjchem-1251	258	25	,	,	PUNCT
eurjchem-1251	258	26	2931	2931	NUM
eurjchem-1251	258	27	,	,	PUNCT
eurjchem-1251	258	28	2877	2877	NUM
eurjchem-1251	258	29	(	(	PUNCT
eurjchem-1251	258	30	ch	ch	NOUN
eurjchem-1251	258	31	aliph	aliph	PROPN
eurjchem-1251	258	32	.	.	PUNCT
eurjchem-1251	258	33	)	)	PUNCT
eurjchem-1251	258	34	,	,	PUNCT
eurjchem-1251	258	35	1311	1311	NUM
eurjchem-1251	258	36	(	(	PUNCT
eurjchem-1251	258	37	so2	so2	PROPN
eurjchem-1251	258	38	,	,	PUNCT
eurjchem-1251	258	39	asym	asym	PROPN
eurjchem-1251	258	40	.	.	PROPN
eurjchem-1251	258	41	)	)	PUNCT
eurjchem-1251	258	42	,	,	PUNCT
eurjchem-1251	258	43	1154	1154	NUM
eurjchem-1251	258	44	(	(	PUNCT
eurjchem-1251	258	45	so2	so2	PROPN
eurjchem-1251	258	46	,	,	PUNCT
eurjchem-1251	258	47	sym	sym	NOUN
eurjchem-1251	258	48	.	.	PUNCT
eurjchem-1251	258	49	)	)	PUNCT
eurjchem-1251	258	50	.	.	PUNCT
eurjchem-1251	259	1	1h	1h	NUM
eurjchem-1251	259	2	nmr	nmr	NOUN
eurjchem-1251	259	3	(	(	PUNCT
eurjchem-1251	259	4	300	300	NUM
eurjchem-1251	259	5	mhz	mhz	NOUN
eurjchem-1251	259	6	,	,	PUNCT
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eurjchem-1251	259	8	,	,	PUNCT
eurjchem-1251	259	9	δ	δ	PROPN
eurjchem-1251	259	10	,	,	PUNCT
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eurjchem-1251	259	12	):	):	PUNCT
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eurjchem-1251	259	14	(	(	PUNCT
eurjchem-1251	259	15	s	s	PROPN
eurjchem-1251	259	16	,	,	PUNCT
eurjchem-1251	259	17	2h	2h	NUM
eurjchem-1251	259	18	,	,	PUNCT
eurjchem-1251	259	19	ch2	ch2	PROPN
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eurjchem-1251	259	21	,	,	PUNCT
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eurjchem-1251	259	23	(	(	PUNCT
eurjchem-1251	259	24	s	s	PROPN
eurjchem-1251	259	25	,	,	PUNCT
eurjchem-1251	259	26	1h	1h	NUM
eurjchem-1251	259	27	,	,	PUNCT
eurjchem-1251	259	28	nhso2	nhso2	NOUN
eurjchem-1251	259	29	)	)	PUNCT
eurjchem-1251	259	30	,	,	PUNCT
eurjchem-1251	259	31	6.58‐7.61	6.58‐7.61	NUM
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eurjchem-1251	259	34	,	,	PUNCT
eurjchem-1251	259	35	24h	24h	NOUN
eurjchem-1251	259	36	,	,	PUNCT
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eurjchem-1251	259	38	‐	‐	ADJ
eurjchem-1251	259	39	h	h	NOUN
eurjchem-1251	259	40	)	)	PUNCT
eurjchem-1251	259	41	,	,	PUNCT
eurjchem-1251	259	42	7.63	7.63	NUM
eurjchem-1251	259	43	(	(	PUNCT
eurjchem-1251	259	44	s	s	PROPN
eurjchem-1251	259	45	,	,	PUNCT
eurjchem-1251	259	46	1h	1h	NUM
eurjchem-1251	259	47	,	,	PUNCT
eurjchem-1251	259	48	nh	nh	PROPN
eurjchem-1251	259	49	)	)	PUNCT
eurjchem-1251	259	50	.	.	PUNCT
eurjchem-1251	260	1	ms	ms	NOUN
eurjchem-1251	260	2	(	(	PUNCT
eurjchem-1251	260	3	ei	ei	PROPN
eurjchem-1251	260	4	,	,	PUNCT
eurjchem-1251	260	5	m	m	PROPN
eurjchem-1251	260	6	/	/	SYM
eurjchem-1251	260	7	z	z	PROPN
eurjchem-1251	260	8	(	(	PUNCT
eurjchem-1251	260	9	%	%	NOUN
eurjchem-1251	260	10	)	)	PUNCT
eurjchem-1251	260	11	):	):	PUNCT
eurjchem-1251	260	12	567	567	NUM
eurjchem-1251	260	13	(	(	PUNCT
eurjchem-1251	260	14	[	[	X
eurjchem-1251	260	15	m‐1]+	m‐1]+	X
eurjchem-1251	260	16	,	,	PUNCT
eurjchem-1251	260	17	48.86	48.86	NUM
eurjchem-1251	260	18	)	)	PUNCT
eurjchem-1251	260	19	,	,	PUNCT
eurjchem-1251	260	20	477	477	NUM
eurjchem-1251	260	21	(	(	PUNCT
eurjchem-1251	260	22	3.41	3.41	NUM
eurjchem-1251	260	23	)	)	PUNCT
eurjchem-1251	260	24	,	,	PUNCT
eurjchem-1251	260	25	466	466	NUM
eurjchem-1251	260	26	(	(	PUNCT
eurjchem-1251	260	27	37.50	37.50	NUM
eurjchem-1251	260	28	)	)	PUNCT
eurjchem-1251	260	29	,	,	PUNCT
eurjchem-1251	260	30	216	216	NUM
eurjchem-1251	260	31	deeb	deeb	PROPN
eurjchem-1251	260	32	et	et	PROPN
eurjchem-1251	260	33	al	al	PROPN
eurjchem-1251	260	34	.	.	PUNCT
eurjchem-1251	260	35	/	/	SYM
eurjchem-1251	260	36	european	european	PROPN
eurjchem-1251	260	37	journal	journal	PROPN
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eurjchem-1251	260	39	chemistry	chemistry	NOUN
eurjchem-1251	260	40	6	6	NUM
eurjchem-1251	260	41	(	(	PUNCT
eurjchem-1251	260	42	2	2	NUM
eurjchem-1251	260	43	)	)	PUNCT
eurjchem-1251	260	44	(	(	PUNCT
eurjchem-1251	260	45	2015	2015	NUM
eurjchem-1251	260	46	)	)	PUNCT
eurjchem-1251	260	47	211‐218	211‐218	NUM
eurjchem-1251	260	48	452	452	NUM
eurjchem-1251	260	49	(	(	PUNCT
eurjchem-1251	260	50	29.55	29.55	NUM
eurjchem-1251	260	51	)	)	PUNCT
eurjchem-1251	260	52	,	,	PUNCT
eurjchem-1251	260	53	390	390	NUM
eurjchem-1251	260	54	(	(	PUNCT
eurjchem-1251	260	55	34.09	34.09	NUM
eurjchem-1251	260	56	)	)	PUNCT
eurjchem-1251	260	57	,	,	PUNCT
eurjchem-1251	260	58	362	362	NUM
eurjchem-1251	260	59	(	(	PUNCT
eurjchem-1251	260	60	35.23	35.23	NUM
eurjchem-1251	260	61	)	)	PUNCT
eurjchem-1251	260	62	,	,	PUNCT
eurjchem-1251	260	63	341	341	NUM
eurjchem-1251	260	64	(	(	PUNCT
eurjchem-1251	260	65	11.93	11.93	NUM
eurjchem-1251	260	66	)	)	PUNCT
eurjchem-1251	260	67	,	,	PUNCT
eurjchem-1251	260	68	305	305	NUM
eurjchem-1251	260	69	(	(	PUNCT
eurjchem-1251	260	70	31.25	31.25	NUM
eurjchem-1251	260	71	)	)	PUNCT
eurjchem-1251	260	72	,	,	PUNCT
eurjchem-1251	260	73	288	288	NUM
eurjchem-1251	260	74	(	(	PUNCT
eurjchem-1251	260	75	37.50	37.50	NUM
eurjchem-1251	260	76	)	)	PUNCT
eurjchem-1251	260	77	,	,	PUNCT
eurjchem-1251	260	78	260	260	NUM
eurjchem-1251	260	79	(	(	PUNCT
eurjchem-1251	260	80	47.73	47.73	NUM
eurjchem-1251	260	81	)	)	PUNCT
eurjchem-1251	260	82	,	,	PUNCT
eurjchem-1251	260	83	234	234	NUM
eurjchem-1251	260	84	(	(	PUNCT
eurjchem-1251	260	85	52.27	52.27	NUM
eurjchem-1251	260	86	)	)	PUNCT
eurjchem-1251	260	87	,	,	PUNCT
eurjchem-1251	260	88	179(43.18	179(43.18	NUM
eurjchem-1251	260	89	)	)	PUNCT
eurjchem-1251	260	90	,	,	PUNCT
eurjchem-1251	260	91	170	170	NUM
eurjchem-1251	260	92	(	(	PUNCT
eurjchem-1251	260	93	31.25	31.25	NUM
eurjchem-1251	260	94	)	)	PUNCT
eurjchem-1251	260	95	,	,	PUNCT
eurjchem-1251	260	96	116	116	NUM
eurjchem-1251	260	97	(	(	PUNCT
eurjchem-1251	260	98	36.93	36.93	NUM
eurjchem-1251	260	99	)	)	PUNCT
eurjchem-1251	260	100	,	,	PUNCT
eurjchem-1251	260	101	106	106	NUM
eurjchem-1251	260	102	(	(	PUNCT
eurjchem-1251	260	103	69.89	69.89	NUM
eurjchem-1251	260	104	)	)	PUNCT
eurjchem-1251	260	105	,	,	PUNCT
eurjchem-1251	260	106	103	103	NUM
eurjchem-1251	260	107	(	(	PUNCT
eurjchem-1251	260	108	44.89	44.89	NUM
eurjchem-1251	260	109	)	)	PUNCT
eurjchem-1251	260	110	,	,	PUNCT
eurjchem-1251	260	111	93	93	NUM
eurjchem-1251	260	112	(	(	PUNCT
eurjchem-1251	260	113	100	100	NUM
eurjchem-1251	260	114	)	)	PUNCT
eurjchem-1251	260	115	,	,	PUNCT
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eurjchem-1251	260	117	(	(	PUNCT
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eurjchem-1251	260	119	)	)	PUNCT
eurjchem-1251	260	120	,	,	PUNCT
eurjchem-1251	260	121	77	77	NUM
eurjchem-1251	260	122	(	(	PUNCT
eurjchem-1251	260	123	16.48	16.48	NUM
eurjchem-1251	260	124	)	)	PUNCT
eurjchem-1251	260	125	.	.	PUNCT
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eurjchem-1251	261	2	.	.	PUNCT
eurjchem-1251	261	3	calcd	calcd	NOUN
eurjchem-1251	261	4	.	.	PUNCT
eurjchem-1251	262	1	for	for	ADP
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eurjchem-1251	262	3	:	:	PUNCT
eurjchem-1251	262	4	c	c	X
eurjchem-1251	262	5	,	,	PUNCT
eurjchem-1251	262	6	73.92	73.92	NUM
eurjchem-1251	262	7	;	;	PUNCT
eurjchem-1251	262	8	h	h	NOUN
eurjchem-1251	262	9	,	,	PUNCT
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eurjchem-1251	262	11	;	;	PUNCT
eurjchem-1251	262	12	n	n	CCONJ
eurjchem-1251	262	13	,	,	PUNCT
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eurjchem-1251	262	15	:	:	PUNCT
eurjchem-1251	263	1	c	c	X
eurjchem-1251	263	2	,	,	PUNCT
eurjchem-1251	263	3	73.60	73.60	NUM
eurjchem-1251	263	4	;	;	PUNCT
eurjchem-1251	263	5	h	h	NOUN
eurjchem-1251	263	6	,	,	PUNCT
eurjchem-1251	263	7	4.80	4.80	NUM
eurjchem-1251	263	8	;	;	PUNCT
eurjchem-1251	263	9	n	n	CCONJ
eurjchem-1251	263	10	,	,	PUNCT
eurjchem-1251	263	11	10.10	10.10	NUM
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eurjchem-1251	263	13	.	.	PUNCT
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eurjchem-1251	264	2	,	,	PUNCT
eurjchem-1251	264	3	5	5	NUM
eurjchem-1251	264	4	,	,	PUNCT
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eurjchem-1251	264	7	(	(	PUNCT
eurjchem-1251	264	8	15c	15c	NOUN
eurjchem-1251	264	9	):	):	PUNCT
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eurjchem-1251	264	11	:	:	PUNCT
eurjchem-1251	264	12	white	white	ADJ
eurjchem-1251	264	13	.	.	PUNCT
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eurjchem-1251	265	2	:	:	PUNCT
eurjchem-1251	265	3	80.35	80.35	NUM
eurjchem-1251	265	4	%	%	NOUN
eurjchem-1251	265	5	.	.	PUNCT
eurjchem-1251	266	1	m.p	m.p	PROPN
eurjchem-1251	266	2	.	.	PROPN
eurjchem-1251	266	3	:	:	PUNCT
eurjchem-1251	267	1	191‐193	191‐193	NUM
eurjchem-1251	267	2	°	°	PROPN
eurjchem-1251	267	3	c	c	X
eurjchem-1251	267	4	.	.	PUNCT
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eurjchem-1251	268	2	(	(	PUNCT
eurjchem-1251	268	3	kbr	kbr	PROPN
eurjchem-1251	268	4	,	,	PUNCT
eurjchem-1251	268	5	ν	ν	PROPN
eurjchem-1251	268	6	,	,	PUNCT
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eurjchem-1251	268	8	):	):	PUNCT
eurjchem-1251	268	9	3349	3349	NUM
eurjchem-1251	268	10	,	,	PUNCT
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eurjchem-1251	268	12	(	(	PUNCT
eurjchem-1251	268	13	2nh	2nh	NOUN
eurjchem-1251	268	14	)	)	PUNCT
eurjchem-1251	268	15	,	,	PUNCT
eurjchem-1251	268	16	3068	3068	NUM
eurjchem-1251	268	17	(	(	PUNCT
eurjchem-1251	268	18	ch	ch	NOUN
eurjchem-1251	268	19	arom	arom	NOUN
eurjchem-1251	268	20	.	.	PUNCT
eurjchem-1251	268	21	)	)	PUNCT
eurjchem-1251	268	22	,	,	PUNCT
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eurjchem-1251	268	24	(	(	PUNCT
eurjchem-1251	268	25	so2	so2	PROPN
eurjchem-1251	268	26	asym	asym	PROPN
eurjchem-1251	268	27	.	.	PROPN
eurjchem-1251	268	28	)	)	PUNCT
eurjchem-1251	268	29	,	,	PUNCT
eurjchem-1251	268	30	1154	1154	NUM
eurjchem-1251	268	31	(	(	PUNCT
eurjchem-1251	268	32	so2	so2	PROPN
eurjchem-1251	268	33	sym	sym	PROPN
eurjchem-1251	268	34	.	.	PUNCT
eurjchem-1251	268	35	)	)	PUNCT
eurjchem-1251	268	36	.	.	PUNCT
eurjchem-1251	269	1	1h	1h	NUM
eurjchem-1251	269	2	nmr	nmr	NOUN
eurjchem-1251	269	3	(	(	PUNCT
eurjchem-1251	269	4	300	300	NUM
eurjchem-1251	269	5	mhz	mhz	NOUN
eurjchem-1251	269	6	,	,	PUNCT
eurjchem-1251	269	7	dmso‐	dmso‐	NUM
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eurjchem-1251	269	9	,	,	PUNCT
eurjchem-1251	269	10	δ	δ	PROPN
eurjchem-1251	269	11	,	,	PUNCT
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eurjchem-1251	269	13	):	):	PUNCT
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eurjchem-1251	269	17	,	,	PUNCT
eurjchem-1251	269	18	1h	1h	NUM
eurjchem-1251	269	19	,	,	PUNCT
eurjchem-1251	269	20	nh	nh	PROPN
eurjchem-1251	269	21	)	)	PUNCT
eurjchem-1251	269	22	,	,	PUNCT
eurjchem-1251	269	23	6.51‐7.39	6.51‐7.39	NUM
eurjchem-1251	269	24	(	(	PUNCT
eurjchem-1251	269	25	m	m	PROPN
eurjchem-1251	269	26	,	,	PUNCT
eurjchem-1251	269	27	24h	24h	NOUN
eurjchem-1251	269	28	,	,	PUNCT
eurjchem-1251	269	29	ar‐h	ar‐h	NOUN
eurjchem-1251	269	30	)	)	PUNCT
eurjchem-1251	269	31	,	,	PUNCT
eurjchem-1251	269	32	9.82	9.82	NUM
eurjchem-1251	269	33	(	(	PUNCT
eurjchem-1251	269	34	s	s	PROPN
eurjchem-1251	269	35	,	,	PUNCT
eurjchem-1251	269	36	1h	1h	NUM
eurjchem-1251	269	37	,	,	PUNCT
eurjchem-1251	269	38	nhso2	nhso2	NOUN
eurjchem-1251	269	39	)	)	PUNCT
eurjchem-1251	269	40	.	.	PUNCT
eurjchem-1251	270	1	ms	ms	NOUN
eurjchem-1251	270	2	(	(	PUNCT
eurjchem-1251	270	3	ei	ei	PROPN
eurjchem-1251	270	4	,	,	PUNCT
eurjchem-1251	270	5	m	m	PROPN
eurjchem-1251	270	6	/	/	SYM
eurjchem-1251	270	7	z	z	PROPN
eurjchem-1251	270	8	(	(	PUNCT
eurjchem-1251	270	9	%	%	NOUN
eurjchem-1251	270	10	)	)	PUNCT
eurjchem-1251	270	11	):	):	PUNCT
eurjchem-1251	270	12	554	554	NUM
eurjchem-1251	270	13	(	(	PUNCT
eurjchem-1251	270	14	m+	m+	NUM
eurjchem-1251	270	15	,	,	PUNCT
eurjchem-1251	270	16	22.10	22.10	NUM
eurjchem-1251	270	17	)	)	PUNCT
eurjchem-1251	270	18	,	,	PUNCT
eurjchem-1251	270	19	462	462	NUM
eurjchem-1251	270	20	(	(	PUNCT
eurjchem-1251	270	21	25.21	25.21	NUM
eurjchem-1251	270	22	)	)	PUNCT
eurjchem-1251	270	23	,	,	PUNCT
eurjchem-1251	270	24	399	399	NUM
eurjchem-1251	270	25	(	(	PUNCT
eurjchem-1251	270	26	4.53	4.53	NUM
eurjchem-1251	270	27	)	)	PUNCT
eurjchem-1251	270	28	,	,	PUNCT
eurjchem-1251	270	29	376	376	NUM
eurjchem-1251	270	30	(	(	PUNCT
eurjchem-1251	270	31	15.58	15.58	NUM
eurjchem-1251	270	32	)	)	PUNCT
eurjchem-1251	270	33	,	,	PUNCT
eurjchem-1251	270	34	350	350	NUM
eurjchem-1251	270	35	(	(	PUNCT
eurjchem-1251	270	36	20.96	20.96	NUM
eurjchem-1251	270	37	)	)	PUNCT
eurjchem-1251	270	38	,	,	PUNCT
eurjchem-1251	270	39	326	326	NUM
eurjchem-1251	270	40	(	(	PUNCT
eurjchem-1251	270	41	19.83	19.83	NUM
eurjchem-1251	270	42	)	)	PUNCT
eurjchem-1251	270	43	,	,	PUNCT
eurjchem-1251	270	44	306	306	NUM
eurjchem-1251	270	45	(	(	PUNCT
eurjchem-1251	270	46	17.56	17.56	NUM
eurjchem-1251	270	47	)	)	PUNCT
eurjchem-1251	270	48	,	,	PUNCT
eurjchem-1251	270	49	245	245	NUM
eurjchem-1251	270	50	(	(	PUNCT
eurjchem-1251	270	51	16.43	16.43	NUM
eurjchem-1251	270	52	)	)	PUNCT
eurjchem-1251	270	53	,	,	PUNCT
eurjchem-1251	270	54	206	206	NUM
eurjchem-1251	270	55	(	(	PUNCT
eurjchem-1251	270	56	18.41	18.41	NUM
eurjchem-1251	270	57	)	)	PUNCT
eurjchem-1251	270	58	,	,	PUNCT
eurjchem-1251	270	59	178	178	NUM
eurjchem-1251	270	60	(	(	PUNCT
eurjchem-1251	270	61	12.18	12.18	NUM
eurjchem-1251	270	62	)	)	PUNCT
eurjchem-1251	270	63	,	,	PUNCT
eurjchem-1251	270	64	154	154	NUM
eurjchem-1251	270	65	(	(	PUNCT
eurjchem-1251	270	66	18.13	18.13	NUM
eurjchem-1251	270	67	)	)	PUNCT
eurjchem-1251	270	68	,	,	PUNCT
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eurjchem-1251	270	70	(	(	PUNCT
eurjchem-1251	270	71	7.65	7.65	NUM
eurjchem-1251	270	72	)	)	PUNCT
eurjchem-1251	270	73	,	,	PUNCT
eurjchem-1251	270	74	107	107	NUM
eurjchem-1251	270	75	(	(	PUNCT
eurjchem-1251	270	76	100	100	NUM
eurjchem-1251	270	77	)	)	PUNCT
eurjchem-1251	270	78	.	.	PUNCT
eurjchem-1251	271	1	anal	anal	PROPN
eurjchem-1251	271	2	.	.	PUNCT
eurjchem-1251	271	3	calcd	calcd	NOUN
eurjchem-1251	271	4	.	.	PUNCT
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eurjchem-1251	272	3	:	:	PUNCT
eurjchem-1251	272	4	c	c	X
eurjchem-1251	272	5	,	,	PUNCT
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eurjchem-1251	272	7	;	;	PUNCT
eurjchem-1251	272	8	h	h	NOUN
eurjchem-1251	272	9	,	,	PUNCT
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eurjchem-1251	272	11	;	;	PUNCT
eurjchem-1251	272	12	n	n	CCONJ
eurjchem-1251	272	13	,	,	PUNCT
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eurjchem-1251	272	15	.	.	PUNCT
eurjchem-1251	272	16	found	find	VERB
eurjchem-1251	272	17	:	:	PUNCT
eurjchem-1251	273	1	c	c	X
eurjchem-1251	273	2	,	,	PUNCT
eurjchem-1251	273	3	73.90	73.90	NUM
eurjchem-1251	273	4	;	;	PUNCT
eurjchem-1251	273	5	h	h	NOUN
eurjchem-1251	273	6	,	,	PUNCT
eurjchem-1251	273	7	4.90	4.90	NUM
eurjchem-1251	273	8	;	;	PUNCT
eurjchem-1251	273	9	n	n	CCONJ
eurjchem-1251	273	10	,	,	PUNCT
eurjchem-1251	273	11	9.80	9.80	NUM
eurjchem-1251	273	12	%	%	NOUN
eurjchem-1251	273	13	.	.	PUNCT
eurjchem-1251	274	1	n‐4‐tolyl‐4‐[(4	n‐4‐tolyl‐4‐[(4	CCONJ
eurjchem-1251	274	2	,	,	PUNCT
eurjchem-1251	274	3	5	5	NUM
eurjchem-1251	274	4	,	,	PUNCT
eurjchem-1251	274	5	6‐triphenylpyridazin‐3‐yl)amino]benzene	6‐triphenylpyridazin‐3‐yl)amino]benzene	NOUN
eurjchem-1251	274	6	sulfonamide	sulfonamide	NOUN
eurjchem-1251	274	7	(	(	PUNCT
eurjchem-1251	274	8	15d	15d	NUM
eurjchem-1251	274	9	):	):	PUNCT
eurjchem-1251	274	10	color	color	NOUN
eurjchem-1251	274	11	:	:	PUNCT
eurjchem-1251	274	12	white	white	ADJ
eurjchem-1251	274	13	.	.	PUNCT
eurjchem-1251	274	14	yield	yield	NOUN
eurjchem-1251	274	15	:	:	PUNCT
eurjchem-1251	274	16	84.4	84.4	NUM
eurjchem-1251	274	17	%	%	NOUN
eurjchem-1251	274	18	.	.	PUNCT
eurjchem-1251	275	1	m.p	m.p	PROPN
eurjchem-1251	275	2	.	.	PROPN
eurjchem-1251	275	3	:	:	PUNCT
eurjchem-1251	276	1	188‐190	188‐190	NUM
eurjchem-1251	276	2	°	°	ADP
eurjchem-1251	276	3	c	c	X
eurjchem-1251	276	4	.	.	PUNCT
eurjchem-1251	277	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	277	2	(	(	PUNCT
eurjchem-1251	277	3	kbr	kbr	PROPN
eurjchem-1251	277	4	,	,	PUNCT
eurjchem-1251	277	5	ν	ν	PROPN
eurjchem-1251	277	6	,	,	PUNCT
eurjchem-1251	277	7	cm‐1	cm‐1	PROPN
eurjchem-1251	277	8	):	):	PUNCT
eurjchem-1251	277	9	3344	3344	NUM
eurjchem-1251	277	10	,	,	PUNCT
eurjchem-1251	277	11	3128	3128	NUM
eurjchem-1251	277	12	(	(	PUNCT
eurjchem-1251	277	13	2nh	2nh	NOUN
eurjchem-1251	277	14	)	)	PUNCT
eurjchem-1251	277	15	,	,	PUNCT
eurjchem-1251	277	16	3064	3064	NUM
eurjchem-1251	277	17	(	(	PUNCT
eurjchem-1251	277	18	ch	ch	NOUN
eurjchem-1251	277	19	arom	arom	NOUN
eurjchem-1251	277	20	.	.	PUNCT
eurjchem-1251	277	21	)	)	PUNCT
eurjchem-1251	277	22	,	,	PUNCT
eurjchem-1251	277	23	2918	2918	NUM
eurjchem-1251	277	24	,	,	PUNCT
eurjchem-1251	277	25	2857	2857	NUM
eurjchem-1251	277	26	(	(	PUNCT
eurjchem-1251	277	27	ch	ch	NOUN
eurjchem-1251	277	28	aliph	aliph	PROPN
eurjchem-1251	277	29	.	.	PUNCT
eurjchem-1251	277	30	)	)	PUNCT
eurjchem-1251	277	31	,	,	PUNCT
eurjchem-1251	277	32	1320	1320	NUM
eurjchem-1251	277	33	(	(	PUNCT
eurjchem-1251	277	34	so2	so2	PROPN
eurjchem-1251	277	35	asym	asym	PROPN
eurjchem-1251	277	36	.	.	PROPN
eurjchem-1251	277	37	)	)	PUNCT
eurjchem-1251	277	38	,	,	PUNCT
eurjchem-1251	277	39	1152	1152	NUM
eurjchem-1251	277	40	(	(	PUNCT
eurjchem-1251	277	41	so2	so2	PROPN
eurjchem-1251	277	42	sym	sym	PROPN
eurjchem-1251	277	43	.	.	PUNCT
eurjchem-1251	277	44	)	)	PUNCT
eurjchem-1251	277	45	.	.	PUNCT
eurjchem-1251	278	1	1h	1h	NUM
eurjchem-1251	278	2	nmr	nmr	NOUN
eurjchem-1251	278	3	(	(	PUNCT
eurjchem-1251	278	4	300	300	NUM
eurjchem-1251	278	5	mhz	mhz	NOUN
eurjchem-1251	278	6	,	,	PUNCT
eurjchem-1251	278	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	278	8	,	,	PUNCT
eurjchem-1251	278	9	δ	δ	PROPN
eurjchem-1251	278	10	,	,	PUNCT
eurjchem-1251	278	11	ppm	ppm	NUM
eurjchem-1251	278	12	):	):	PUNCT
eurjchem-1251	278	13	2.17	2.17	NUM
eurjchem-1251	278	14	(	(	PUNCT
eurjchem-1251	278	15	s	s	PROPN
eurjchem-1251	278	16	,	,	PUNCT
eurjchem-1251	278	17	3h	3h	NUM
eurjchem-1251	278	18	,	,	PUNCT
eurjchem-1251	278	19	ch3	ch3	PROPN
eurjchem-1251	278	20	)	)	PUNCT
eurjchem-1251	278	21	,	,	PUNCT
eurjchem-1251	278	22	5.91	5.91	NUM
eurjchem-1251	278	23	(	(	PUNCT
eurjchem-1251	278	24	s	s	PROPN
eurjchem-1251	278	25	,	,	PUNCT
eurjchem-1251	278	26	1h	1h	NUM
eurjchem-1251	278	27	,	,	PUNCT
eurjchem-1251	278	28	nh	nh	PROPN
eurjchem-1251	278	29	)	)	PUNCT
eurjchem-1251	278	30	,	,	PUNCT
eurjchem-1251	278	31	6.49‐7.37	6.49‐7.37	NUM
eurjchem-1251	278	32	(	(	PUNCT
eurjchem-1251	278	33	m	m	PROPN
eurjchem-1251	278	34	,	,	PUNCT
eurjchem-1251	278	35	23h	23h	NOUN
eurjchem-1251	278	36	,	,	PUNCT
eurjchem-1251	278	37	ar‐h	ar‐h	PROPN
eurjchem-1251	278	38	)	)	PUNCT
eurjchem-1251	278	39	,	,	PUNCT
eurjchem-1251	278	40	9.64	9.64	NUM
eurjchem-1251	278	41	(	(	PUNCT
eurjchem-1251	278	42	s	s	PROPN
eurjchem-1251	278	43	,	,	PUNCT
eurjchem-1251	278	44	1h	1h	NUM
eurjchem-1251	278	45	,	,	PUNCT
eurjchem-1251	278	46	nhso2	nhso2	NOUN
eurjchem-1251	278	47	)	)	PUNCT
eurjchem-1251	278	48	.	.	PUNCT
eurjchem-1251	279	1	ms	ms	NOUN
eurjchem-1251	279	2	(	(	PUNCT
eurjchem-1251	279	3	ei	ei	PROPN
eurjchem-1251	279	4	,	,	PUNCT
eurjchem-1251	279	5	m	m	PROPN
eurjchem-1251	279	6	/	/	SYM
eurjchem-1251	279	7	z	z	PROPN
eurjchem-1251	279	8	(	(	PUNCT
eurjchem-1251	279	9	%	%	NOUN
eurjchem-1251	279	10	)	)	PUNCT
eurjchem-1251	279	11	):	):	PUNCT
eurjchem-1251	279	12	568	568	NUM
eurjchem-1251	279	13	(	(	PUNCT
eurjchem-1251	279	14	m+	m+	NUM
eurjchem-1251	279	15	,	,	PUNCT
eurjchem-1251	279	16	74.00	74.00	NUM
eurjchem-1251	279	17	)	)	PUNCT
eurjchem-1251	279	18	,	,	PUNCT
eurjchem-1251	279	19	540	540	NUM
eurjchem-1251	279	20	(	(	PUNCT
eurjchem-1251	279	21	54.00	54.00	NUM
eurjchem-1251	279	22	)	)	PUNCT
eurjchem-1251	279	23	,	,	PUNCT
eurjchem-1251	279	24	526	526	NUM
eurjchem-1251	279	25	(	(	PUNCT
eurjchem-1251	279	26	65.00	65.00	NUM
eurjchem-1251	279	27	)	)	PUNCT
eurjchem-1251	279	28	,	,	PUNCT
eurjchem-1251	279	29	477	477	NUM
eurjchem-1251	279	30	(	(	PUNCT
eurjchem-1251	279	31	65.00	65.00	NUM
eurjchem-1251	279	32	)	)	PUNCT
eurjchem-1251	279	33	,	,	PUNCT
eurjchem-1251	279	34	450	450	NUM
eurjchem-1251	279	35	(	(	PUNCT
eurjchem-1251	279	36	84.00	84.00	NUM
eurjchem-1251	279	37	)	)	PUNCT
eurjchem-1251	279	38	,	,	PUNCT
eurjchem-1251	279	39	435	435	NUM
eurjchem-1251	279	40	(	(	PUNCT
eurjchem-1251	279	41	84.00	84.00	NUM
eurjchem-1251	279	42	)	)	PUNCT
eurjchem-1251	279	43	,	,	PUNCT
eurjchem-1251	279	44	401	401	NUM
eurjchem-1251	279	45	(	(	PUNCT
eurjchem-1251	279	46	100	100	NUM
eurjchem-1251	279	47	)	)	PUNCT
eurjchem-1251	279	48	,	,	PUNCT
eurjchem-1251	279	49	399	399	NUM
eurjchem-1251	279	50	(	(	PUNCT
eurjchem-1251	279	51	58.00	58.00	NUM
eurjchem-1251	279	52	)	)	PUNCT
eurjchem-1251	279	53	,	,	PUNCT
eurjchem-1251	279	54	388	388	NUM
eurjchem-1251	279	55	(	(	PUNCT
eurjchem-1251	279	56	54.00	54.00	NUM
eurjchem-1251	279	57	)	)	PUNCT
eurjchem-1251	279	58	,	,	PUNCT
eurjchem-1251	279	59	312	312	NUM
eurjchem-1251	279	60	(	(	PUNCT
eurjchem-1251	279	61	55.00	55.00	NUM
eurjchem-1251	279	62	)	)	PUNCT
eurjchem-1251	279	63	,	,	PUNCT
eurjchem-1251	279	64	308	308	NUM
eurjchem-1251	279	65	(	(	PUNCT
eurjchem-1251	279	66	57.00	57.00	NUM
eurjchem-1251	279	67	)	)	PUNCT
eurjchem-1251	279	68	,	,	PUNCT
eurjchem-1251	279	69	279	279	NUM
eurjchem-1251	279	70	(	(	PUNCT
eurjchem-1251	279	71	6.00	6.00	NUM
eurjchem-1251	279	72	)	)	PUNCT
eurjchem-1251	279	73	,	,	PUNCT
eurjchem-1251	279	74	261	261	NUM
eurjchem-1251	279	75	(	(	PUNCT
eurjchem-1251	279	76	71.00	71.00	NUM
eurjchem-1251	279	77	)	)	PUNCT
eurjchem-1251	279	78	,	,	PUNCT
eurjchem-1251	279	79	169	169	NUM
eurjchem-1251	279	80	(	(	PUNCT
eurjchem-1251	279	81	78.00	78.00	NUM
eurjchem-1251	279	82	)	)	PUNCT
eurjchem-1251	279	83	,	,	PUNCT
eurjchem-1251	279	84	105	105	NUM
eurjchem-1251	279	85	(	(	PUNCT
eurjchem-1251	279	86	57.00	57.00	NUM
eurjchem-1251	279	87	)	)	PUNCT
eurjchem-1251	279	88	,	,	PUNCT
eurjchem-1251	279	89	76	76	NUM
eurjchem-1251	279	90	(	(	PUNCT
eurjchem-1251	279	91	82.00	82.00	NUM
eurjchem-1251	279	92	)	)	PUNCT
eurjchem-1251	279	93	.	.	PUNCT
eurjchem-1251	280	1	anal	anal	PROPN
eurjchem-1251	280	2	.	.	PUNCT
eurjchem-1251	280	3	calcd	calcd	NOUN
eurjchem-1251	280	4	.	.	PUNCT
eurjchem-1251	281	1	for	for	SCONJ
eurjchem-1251	281	2	c35h28n4o2s	c35h28n4o2s	PROPN
eurjchem-1251	281	3	:	:	PUNCT
eurjchem-1251	281	4	c	c	X
eurjchem-1251	281	5	,	,	PUNCT
eurjchem-1251	281	6	73.92	73.92	NUM
eurjchem-1251	281	7	;	;	PUNCT
eurjchem-1251	281	8	h	h	NOUN
eurjchem-1251	281	9	,	,	PUNCT
eurjchem-1251	281	10	4.96	4.96	NUM
eurjchem-1251	281	11	;	;	PUNCT
eurjchem-1251	281	12	n	n	CCONJ
eurjchem-1251	281	13	,	,	PUNCT
eurjchem-1251	281	14	9.85	9.85	NUM
eurjchem-1251	281	15	.	.	PUNCT
eurjchem-1251	281	16	found	find	VERB
eurjchem-1251	281	17	:	:	PUNCT
eurjchem-1251	282	1	c	c	X
eurjchem-1251	282	2	,	,	PUNCT
eurjchem-1251	282	3	73.60	73.60	NUM
eurjchem-1251	282	4	;	;	PUNCT
eurjchem-1251	282	5	h	h	NOUN
eurjchem-1251	282	6	,	,	PUNCT
eurjchem-1251	282	7	5.10	5.10	NUM
eurjchem-1251	282	8	;	;	PUNCT
eurjchem-1251	282	9	n	n	CCONJ
eurjchem-1251	282	10	,	,	PUNCT
eurjchem-1251	282	11	9.60	9.60	NUM
eurjchem-1251	282	12	%	%	NOUN
eurjchem-1251	282	13	.	.	PUNCT
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eurjchem-1251	283	2	,	,	PUNCT
eurjchem-1251	283	3	5	5	NUM
eurjchem-1251	283	4	,	,	PUNCT
eurjchem-1251	283	5	6‐triphenylpyridazin‐3‐yl	6‐triphenylpyridazin‐3‐yl	NUM
eurjchem-1251	283	6	)	)	PUNCT
eurjchem-1251	283	7	amino]benzenesulfonamide	amino]benzenesulfonamide	PROPN
eurjchem-1251	283	8	(	(	PUNCT
eurjchem-1251	283	9	15e	15e	NOUN
eurjchem-1251	283	10	):	):	PUNCT
eurjchem-1251	283	11	color	color	NOUN
eurjchem-1251	283	12	:	:	PUNCT
eurjchem-1251	283	13	white	white	ADJ
eurjchem-1251	283	14	.	.	PUNCT
eurjchem-1251	283	15	yield	yield	NOUN
eurjchem-1251	283	16	:	:	PUNCT
eurjchem-1251	283	17	86.75	86.75	NUM
eurjchem-1251	283	18	%	%	NOUN
eurjchem-1251	283	19	.	.	PUNCT
eurjchem-1251	284	1	m.p	m.p	PROPN
eurjchem-1251	284	2	.	.	PROPN
eurjchem-1251	284	3	:	:	PUNCT
eurjchem-1251	285	1	198‐200	198‐200	NUM
eurjchem-1251	285	2	°	°	PROPN
eurjchem-1251	285	3	c	c	X
eurjchem-1251	285	4	.	.	PUNCT
eurjchem-1251	286	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	286	2	(	(	PUNCT
eurjchem-1251	286	3	kbr	kbr	PROPN
eurjchem-1251	286	4	,	,	PUNCT
eurjchem-1251	286	5	ν	ν	PROPN
eurjchem-1251	286	6	,	,	PUNCT
eurjchem-1251	286	7	cm‐1	cm‐1	PROPN
eurjchem-1251	286	8	):	):	PUNCT
eurjchem-1251	286	9	3388	3388	NUM
eurjchem-1251	286	10	,	,	PUNCT
eurjchem-1251	286	11	3282	3282	NUM
eurjchem-1251	286	12	(	(	PUNCT
eurjchem-1251	286	13	2	2	NUM
eurjchem-1251	286	14	nh	nh	NOUN
eurjchem-1251	286	15	)	)	PUNCT
eurjchem-1251	286	16	,	,	PUNCT
eurjchem-1251	286	17	3074	3074	NUM
eurjchem-1251	286	18	(	(	PUNCT
eurjchem-1251	286	19	ch	ch	NOUN
eurjchem-1251	286	20	arom	arom	NOUN
eurjchem-1251	286	21	.	.	PUNCT
eurjchem-1251	286	22	)	)	PUNCT
eurjchem-1251	286	23	,	,	PUNCT
eurjchem-1251	286	24	2957	2957	NUM
eurjchem-1251	286	25	,	,	PUNCT
eurjchem-1251	286	26	2835	2835	NUM
eurjchem-1251	286	27	(	(	PUNCT
eurjchem-1251	286	28	ch	ch	NOUN
eurjchem-1251	286	29	aliph	aliph	PROPN
eurjchem-1251	286	30	.	.	PUNCT
eurjchem-1251	286	31	)	)	PUNCT
eurjchem-1251	286	32	,	,	PUNCT
eurjchem-1251	286	33	1310	1310	NUM
eurjchem-1251	286	34	(	(	PUNCT
eurjchem-1251	286	35	so2	so2	PROPN
eurjchem-1251	286	36	asym	asym	PROPN
eurjchem-1251	286	37	.	.	PROPN
eurjchem-1251	286	38	)	)	PUNCT
eurjchem-1251	286	39	,	,	PUNCT
eurjchem-1251	286	40	1252	1252	NUM
eurjchem-1251	286	41	(	(	PUNCT
eurjchem-1251	286	42	c	c	X
eurjchem-1251	286	43	–	–	PUNCT
eurjchem-1251	286	44	o	o	NOUN
eurjchem-1251	286	45	)	)	PUNCT
eurjchem-1251	286	46	,	,	PUNCT
eurjchem-1251	286	47	1148	1148	NUM
eurjchem-1251	286	48	(	(	PUNCT
eurjchem-1251	286	49	so2	so2	PROPN
eurjchem-1251	286	50	,	,	PUNCT
eurjchem-1251	286	51	sym	sym	NOUN
eurjchem-1251	286	52	,	,	PUNCT
eurjchem-1251	286	53	)	)	PUNCT
eurjchem-1251	286	54	.	.	PUNCT
eurjchem-1251	287	1	1h	1h	NUM
eurjchem-1251	287	2	nmr	nmr	NOUN
eurjchem-1251	287	3	(	(	PUNCT
eurjchem-1251	287	4	300	300	NUM
eurjchem-1251	287	5	mhz	mhz	NOUN
eurjchem-1251	287	6	,	,	PUNCT
eurjchem-1251	287	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	287	8	,	,	PUNCT
eurjchem-1251	287	9	δ	δ	PROPN
eurjchem-1251	287	10	,	,	PUNCT
eurjchem-1251	287	11	ppm	ppm	NUM
eurjchem-1251	287	12	):	):	PUNCT
eurjchem-1251	287	13	3.66	3.66	NUM
eurjchem-1251	287	14	(	(	PUNCT
eurjchem-1251	287	15	s	s	PROPN
eurjchem-1251	287	16	,	,	PUNCT
eurjchem-1251	287	17	3h	3h	NUM
eurjchem-1251	287	18	,	,	PUNCT
eurjchem-1251	287	19	ch3	ch3	PROPN
eurjchem-1251	287	20	)	)	PUNCT
eurjchem-1251	287	21	,	,	PUNCT
eurjchem-1251	287	22	5.90	5.90	NUM
eurjchem-1251	287	23	(	(	PUNCT
eurjchem-1251	287	24	s	s	PROPN
eurjchem-1251	287	25	,	,	PUNCT
eurjchem-1251	287	26	1h	1h	NUM
eurjchem-1251	287	27	,	,	PUNCT
eurjchem-1251	287	28	nh	nh	PROPN
eurjchem-1251	287	29	)	)	PUNCT
eurjchem-1251	287	30	,	,	PUNCT
eurjchem-1251	287	31	6.48‐7.32	6.48‐7.32	NUM
eurjchem-1251	287	32	(	(	PUNCT
eurjchem-1251	287	33	m	m	PROPN
eurjchem-1251	287	34	,	,	PUNCT
eurjchem-1251	287	35	23h	23h	NOUN
eurjchem-1251	287	36	,	,	PUNCT
eurjchem-1251	287	37	ar‐h	ar‐h	PROPN
eurjchem-1251	287	38	)	)	PUNCT
eurjchem-1251	287	39	,	,	PUNCT
eurjchem-1251	287	40	9.43	9.43	NUM
eurjchem-1251	287	41	(	(	PUNCT
eurjchem-1251	287	42	s	s	PROPN
eurjchem-1251	287	43	,	,	PUNCT
eurjchem-1251	287	44	1h	1h	NUM
eurjchem-1251	287	45	,	,	PUNCT
eurjchem-1251	287	46	nhso2	nhso2	NOUN
eurjchem-1251	287	47	)	)	PUNCT
eurjchem-1251	287	48	.	.	PUNCT
eurjchem-1251	288	1	ms	ms	NOUN
eurjchem-1251	288	2	(	(	PUNCT
eurjchem-1251	288	3	ei	ei	PROPN
eurjchem-1251	288	4	,	,	PUNCT
eurjchem-1251	288	5	m	m	PROPN
eurjchem-1251	288	6	/	/	SYM
eurjchem-1251	288	7	z	z	PROPN
eurjchem-1251	288	8	(	(	PUNCT
eurjchem-1251	288	9	%	%	NOUN
eurjchem-1251	288	10	)	)	PUNCT
eurjchem-1251	288	11	):	):	PUNCT
eurjchem-1251	288	12	584	584	NUM
eurjchem-1251	288	13	(	(	PUNCT
eurjchem-1251	288	14	m+	m+	NUM
eurjchem-1251	288	15	,	,	PUNCT
eurjchem-1251	288	16	44.78	44.78	NUM
eurjchem-1251	288	17	)	)	PUNCT
eurjchem-1251	288	18	,	,	PUNCT
eurjchem-1251	288	19	554	554	NUM
eurjchem-1251	288	20	(	(	PUNCT
eurjchem-1251	288	21	41.79	41.79	NUM
eurjchem-1251	288	22	)	)	PUNCT
eurjchem-1251	288	23	,	,	PUNCT
eurjchem-1251	288	24	508	508	NUM
eurjchem-1251	288	25	(	(	PUNCT
eurjchem-1251	288	26	28.86	28.86	NUM
eurjchem-1251	288	27	)	)	PUNCT
eurjchem-1251	288	28	,	,	PUNCT
eurjchem-1251	288	29	478	478	NUM
eurjchem-1251	288	30	(	(	PUNCT
eurjchem-1251	288	31	28.36	28.36	NUM
eurjchem-1251	288	32	)	)	PUNCT
eurjchem-1251	288	33	,	,	PUNCT
eurjchem-1251	288	34	463	463	NUM
eurjchem-1251	288	35	(	(	PUNCT
eurjchem-1251	288	36	25.87	25.87	NUM
eurjchem-1251	288	37	)	)	PUNCT
eurjchem-1251	288	38	,	,	PUNCT
eurjchem-1251	288	39	406	406	NUM
eurjchem-1251	288	40	(	(	PUNCT
eurjchem-1251	288	41	41.79	41.79	NUM
eurjchem-1251	288	42	)	)	PUNCT
eurjchem-1251	288	43	,	,	PUNCT
eurjchem-1251	288	44	398	398	NUM
eurjchem-1251	288	45	(	(	PUNCT
eurjchem-1251	288	46	33.83	33.83	NUM
eurjchem-1251	288	47	)	)	PUNCT
eurjchem-1251	288	48	,	,	PUNCT
eurjchem-1251	288	49	377	377	NUM
eurjchem-1251	288	50	(	(	PUNCT
eurjchem-1251	288	51	26.87	26.87	NUM
eurjchem-1251	288	52	)	)	PUNCT
eurjchem-1251	288	53	,	,	PUNCT
eurjchem-1251	288	54	321	321	NUM
eurjchem-1251	288	55	(	(	PUNCT
eurjchem-1251	288	56	28.36	28.36	NUM
eurjchem-1251	288	57	)	)	PUNCT
eurjchem-1251	288	58	,	,	PUNCT
eurjchem-1251	288	59	262	262	NUM
eurjchem-1251	288	60	(	(	PUNCT
eurjchem-1251	288	61	41.79	41.79	NUM
eurjchem-1251	288	62	)	)	PUNCT
eurjchem-1251	288	63	,	,	PUNCT
eurjchem-1251	288	64	206	206	NUM
eurjchem-1251	288	65	(	(	PUNCT
eurjchem-1251	288	66	34.83	34.83	NUM
eurjchem-1251	288	67	)	)	PUNCT
eurjchem-1251	288	68	,	,	PUNCT
eurjchem-1251	288	69	186	186	NUM
eurjchem-1251	288	70	(	(	PUNCT
eurjchem-1251	288	71	28.36	28.36	NUM
eurjchem-1251	288	72	)	)	PUNCT
eurjchem-1251	288	73	,	,	PUNCT
eurjchem-1251	288	74	179	179	NUM
eurjchem-1251	288	75	(	(	PUNCT
eurjchem-1251	288	76	29.85	29.85	NUM
eurjchem-1251	288	77	)	)	PUNCT
eurjchem-1251	288	78	,	,	PUNCT
eurjchem-1251	288	79	123	123	NUM
eurjchem-1251	288	80	(	(	PUNCT
eurjchem-1251	288	81	32.34	32.34	NUM
eurjchem-1251	288	82	)	)	PUNCT
eurjchem-1251	288	83	,	,	PUNCT
eurjchem-1251	288	84	107	107	NUM
eurjchem-1251	288	85	(	(	PUNCT
eurjchem-1251	288	86	80.10	80.10	NUM
eurjchem-1251	288	87	)	)	PUNCT
eurjchem-1251	288	88	,	,	PUNCT
eurjchem-1251	288	89	106	106	NUM
eurjchem-1251	288	90	(	(	PUNCT
eurjchem-1251	288	91	100	100	NUM
eurjchem-1251	288	92	)	)	PUNCT
eurjchem-1251	288	93	,	,	PUNCT
eurjchem-1251	288	94	77	77	NUM
eurjchem-1251	288	95	(	(	PUNCT
eurjchem-1251	288	96	42.79	42.79	NUM
eurjchem-1251	288	97	)	)	PUNCT
eurjchem-1251	288	98	.	.	PUNCT
eurjchem-1251	289	1	anal	anal	PROPN
eurjchem-1251	289	2	.	.	PUNCT
eurjchem-1251	289	3	calcd	calcd	NOUN
eurjchem-1251	289	4	.	.	PUNCT
eurjchem-1251	290	1	for	for	SCONJ
eurjchem-1251	290	2	c35h28n4o3s	c35h28n4o3s	NUM
eurjchem-1251	290	3	:	:	PUNCT
eurjchem-1251	290	4	c	c	X
eurjchem-1251	290	5	,	,	PUNCT
eurjchem-1251	290	6	71.90	71.90	NUM
eurjchem-1251	290	7	;	;	PUNCT
eurjchem-1251	290	8	h	h	NOUN
eurjchem-1251	290	9	,	,	PUNCT
eurjchem-1251	290	10	4.83	4.83	NUM
eurjchem-1251	290	11	;	;	PUNCT
eurjchem-1251	290	12	n	n	CCONJ
eurjchem-1251	290	13	,	,	PUNCT
eurjchem-1251	290	14	9.58	9.58	NUM
eurjchem-1251	290	15	.	.	PUNCT
eurjchem-1251	290	16	found	find	VERB
eurjchem-1251	290	17	:	:	PUNCT
eurjchem-1251	291	1	c	c	X
eurjchem-1251	291	2	,	,	PUNCT
eurjchem-1251	291	3	71.50	71.50	NUM
eurjchem-1251	291	4	;	;	PUNCT
eurjchem-1251	291	5	h	h	NOUN
eurjchem-1251	291	6	,	,	PUNCT
eurjchem-1251	291	7	4.90	4.90	NUM
eurjchem-1251	291	8	;	;	PUNCT
eurjchem-1251	291	9	n	n	CCONJ
eurjchem-1251	291	10	,	,	PUNCT
eurjchem-1251	291	11	9.30	9.30	NUM
eurjchem-1251	291	12	%	%	NOUN
eurjchem-1251	291	13	.	.	PUNCT
eurjchem-1251	292	1	n‐(4‐chlorophenyl)‐4‐[(4	n‐(4‐chlorophenyl)‐4‐[(4	NOUN
eurjchem-1251	292	2	,	,	PUNCT
eurjchem-1251	292	3	5	5	NUM
eurjchem-1251	292	4	,	,	PUNCT
eurjchem-1251	292	5	6‐triphenylpyridazin‐3‐yl	6‐triphenylpyridazin‐3‐yl	NUM
eurjchem-1251	292	6	)	)	PUNCT
eurjchem-1251	292	7	amino]benzenesulfonamide	amino]benzenesulfonamide	PROPN
eurjchem-1251	292	8	(	(	PUNCT
eurjchem-1251	292	9	15f	15f	NOUN
eurjchem-1251	292	10	):	):	PUNCT
eurjchem-1251	292	11	color	color	NOUN
eurjchem-1251	292	12	:	:	PUNCT
eurjchem-1251	292	13	white	white	ADJ
eurjchem-1251	292	14	.	.	PUNCT
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eurjchem-1251	293	2	:	:	PUNCT
eurjchem-1251	293	3	87.3	87.3	NUM
eurjchem-1251	293	4	%	%	NOUN
eurjchem-1251	293	5	.	.	PUNCT
eurjchem-1251	294	1	m.p	m.p	PROPN
eurjchem-1251	294	2	.	.	PROPN
eurjchem-1251	294	3	:	:	PUNCT
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eurjchem-1251	295	2	°	°	PROPN
eurjchem-1251	295	3	c	c	PROPN
eurjchem-1251	295	4	.	.	PUNCT
eurjchem-1251	296	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	296	2	(	(	PUNCT
eurjchem-1251	296	3	kbr	kbr	PROPN
eurjchem-1251	296	4	,	,	PUNCT
eurjchem-1251	296	5	ν	ν	PROPN
eurjchem-1251	296	6	,	,	PUNCT
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eurjchem-1251	296	8	):	):	PUNCT
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eurjchem-1251	296	10	,	,	PUNCT
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eurjchem-1251	296	12	(	(	PUNCT
eurjchem-1251	296	13	2nh	2nh	NOUN
eurjchem-1251	296	14	)	)	PUNCT
eurjchem-1251	296	15	,	,	PUNCT
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eurjchem-1251	296	17	(	(	PUNCT
eurjchem-1251	296	18	ch	ch	NOUN
eurjchem-1251	296	19	aomr	aomr	PROPN
eurjchem-1251	296	20	.	.	PUNCT
eurjchem-1251	296	21	)	)	PUNCT
eurjchem-1251	296	22	,	,	PUNCT
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eurjchem-1251	296	24	(	(	PUNCT
eurjchem-1251	296	25	so2	so2	PROPN
eurjchem-1251	296	26	asym	asym	PROPN
eurjchem-1251	296	27	.	.	PROPN
eurjchem-1251	296	28	)	)	PUNCT
eurjchem-1251	296	29	,	,	PUNCT
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eurjchem-1251	296	31	(	(	PUNCT
eurjchem-1251	296	32	so2	so2	PROPN
eurjchem-1251	296	33	sym	sym	PROPN
eurjchem-1251	296	34	.	.	PUNCT
eurjchem-1251	296	35	)	)	PUNCT
eurjchem-1251	296	36	.	.	PUNCT
eurjchem-1251	297	1	1h	1h	NUM
eurjchem-1251	297	2	nmr	nmr	NOUN
eurjchem-1251	297	3	(	(	PUNCT
eurjchem-1251	297	4	300	300	NUM
eurjchem-1251	297	5	mhz	mhz	NOUN
eurjchem-1251	297	6	,	,	PUNCT
eurjchem-1251	297	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	297	8	,	,	PUNCT
eurjchem-1251	297	9	δ	δ	PROPN
eurjchem-1251	297	10	,	,	PUNCT
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eurjchem-1251	297	12	):	):	PUNCT
eurjchem-1251	297	13	5.98	5.98	NUM
eurjchem-1251	297	14	(	(	PUNCT
eurjchem-1251	297	15	s	s	PROPN
eurjchem-1251	297	16	,	,	PUNCT
eurjchem-1251	297	17	1h	1h	NUM
eurjchem-1251	297	18	,	,	PUNCT
eurjchem-1251	297	19	nh	nh	PROPN
eurjchem-1251	297	20	)	)	PUNCT
eurjchem-1251	297	21	,	,	PUNCT
eurjchem-1251	297	22	6.51‐7.40	6.51‐7.40	NUM
eurjchem-1251	297	23	(	(	PUNCT
eurjchem-1251	297	24	m	m	PROPN
eurjchem-1251	297	25	,	,	PUNCT
eurjchem-1251	297	26	23h	23h	NOUN
eurjchem-1251	297	27	,	,	PUNCT
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eurjchem-1251	297	29	)	)	PUNCT
eurjchem-1251	297	30	,	,	PUNCT
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eurjchem-1251	297	32	(	(	PUNCT
eurjchem-1251	297	33	s	s	PROPN
eurjchem-1251	297	34	,	,	PUNCT
eurjchem-1251	297	35	1h	1h	NUM
eurjchem-1251	297	36	,	,	PUNCT
eurjchem-1251	297	37	nhso2	nhso2	NOUN
eurjchem-1251	297	38	)	)	PUNCT
eurjchem-1251	297	39	.	.	PUNCT
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eurjchem-1251	298	2	(	(	PUNCT
eurjchem-1251	298	3	ei	ei	PROPN
eurjchem-1251	298	4	,	,	PUNCT
eurjchem-1251	298	5	m	m	PROPN
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eurjchem-1251	298	7	z	z	PROPN
eurjchem-1251	298	8	(	(	PUNCT
eurjchem-1251	298	9	%	%	NOUN
eurjchem-1251	298	10	)	)	PUNCT
eurjchem-1251	298	11	):	):	PUNCT
eurjchem-1251	298	12	590.5	590.5	NUM
eurjchem-1251	298	13	(	(	PUNCT
eurjchem-1251	298	14	m++2	m++2	PROPN
eurjchem-1251	298	15	,	,	PUNCT
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eurjchem-1251	298	17	)	)	PUNCT
eurjchem-1251	298	18	,	,	PUNCT
eurjchem-1251	298	19	588.5	588.5	NUM
eurjchem-1251	298	20	(	(	PUNCT
eurjchem-1251	298	21	m+	m+	NUM
eurjchem-1251	298	22	,	,	PUNCT
eurjchem-1251	298	23	2.87	2.87	NUM
eurjchem-1251	298	24	)	)	PUNCT
eurjchem-1251	298	25	,	,	PUNCT
eurjchem-1251	298	26	486	486	NUM
eurjchem-1251	298	27	(	(	PUNCT
eurjchem-1251	298	28	3.08	3.08	NUM
eurjchem-1251	298	29	)	)	PUNCT
eurjchem-1251	298	30	,	,	PUNCT
eurjchem-1251	298	31	477	477	NUM
eurjchem-1251	298	32	(	(	PUNCT
eurjchem-1251	298	33	3.63	3.63	NUM
eurjchem-1251	298	34	)	)	PUNCT
eurjchem-1251	298	35	,	,	PUNCT
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eurjchem-1251	298	37	(	(	PUNCT
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eurjchem-1251	298	39	)	)	PUNCT
eurjchem-1251	298	40	,	,	PUNCT
eurjchem-1251	298	41	282	282	NUM
eurjchem-1251	298	42	(	(	PUNCT
eurjchem-1251	298	43	45.14	45.14	NUM
eurjchem-1251	298	44	)	)	PUNCT
eurjchem-1251	298	45	,	,	PUNCT
eurjchem-1251	298	46	156	156	NUM
eurjchem-1251	298	47	(	(	PUNCT
eurjchem-1251	298	48	100	100	NUM
eurjchem-1251	298	49	)	)	PUNCT
eurjchem-1251	298	50	,	,	PUNCT
eurjchem-1251	298	51	155	155	NUM
eurjchem-1251	298	52	(	(	PUNCT
eurjchem-1251	298	53	19.51	19.51	NUM
eurjchem-1251	298	54	)	)	PUNCT
eurjchem-1251	298	55	,	,	PUNCT
eurjchem-1251	298	56	127	127	NUM
eurjchem-1251	298	57	(	(	PUNCT
eurjchem-1251	298	58	17.78	17.78	NUM
eurjchem-1251	298	59	)	)	PUNCT
eurjchem-1251	298	60	.	.	PUNCT
eurjchem-1251	299	1	anal	anal	PROPN
eurjchem-1251	299	2	.	.	PUNCT
eurjchem-1251	299	3	calcd	calcd	NOUN
eurjchem-1251	299	4	.	.	PUNCT
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eurjchem-1251	300	3	:	:	PUNCT
eurjchem-1251	300	4	c	c	X
eurjchem-1251	300	5	,	,	PUNCT
eurjchem-1251	300	6	69.32	69.32	NUM
eurjchem-1251	300	7	;	;	PUNCT
eurjchem-1251	300	8	h	h	NOUN
eurjchem-1251	300	9	,	,	PUNCT
eurjchem-1251	300	10	4.28	4.28	NUM
eurjchem-1251	300	11	;	;	PUNCT
eurjchem-1251	300	12	n	n	CCONJ
eurjchem-1251	300	13	,	,	PUNCT
eurjchem-1251	300	14	9.51	9.51	NUM
eurjchem-1251	300	15	.	.	PUNCT
eurjchem-1251	300	16	found	find	VERB
eurjchem-1251	300	17	:	:	PUNCT
eurjchem-1251	301	1	c	c	X
eurjchem-1251	301	2	,	,	PUNCT
eurjchem-1251	301	3	69.64	69.64	NUM
eurjchem-1251	301	4	;	;	PUNCT
eurjchem-1251	301	5	h	h	NOUN
eurjchem-1251	301	6	,	,	PUNCT
eurjchem-1251	301	7	4.20	4.20	NUM
eurjchem-1251	301	8	;	;	PUNCT
eurjchem-1251	301	9	n	n	CCONJ
eurjchem-1251	301	10	,	,	PUNCT
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eurjchem-1251	301	12	%	%	NOUN
eurjchem-1251	301	13	.	.	PUNCT
eurjchem-1251	302	1	n‐(4‐nitrophenyl)‐4‐[(4,5,6‐triphenylpyridazin‐3‐yl	n‐(4‐nitrophenyl)‐4‐[(4,5,6‐triphenylpyridazin‐3‐yl	VERB
eurjchem-1251	302	2	)	)	PUNCT
eurjchem-1251	302	3	amino	amino	NOUN
eurjchem-1251	302	4	]	]	PUNCT
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eurjchem-1251	302	6	(	(	PUNCT
eurjchem-1251	302	7	15	15	NUM
eurjchem-1251	302	8	g	g	NOUN
eurjchem-1251	302	9	):	):	PUNCT
eurjchem-1251	302	10	color	color	NOUN
eurjchem-1251	302	11	:	:	PUNCT
eurjchem-1251	302	12	white	white	ADJ
eurjchem-1251	302	13	.	.	PUNCT
eurjchem-1251	303	1	yield	yield	NOUN
eurjchem-1251	303	2	:	:	PUNCT
eurjchem-1251	303	3	91.43	91.43	NUM
eurjchem-1251	303	4	%	%	NOUN
eurjchem-1251	303	5	.	.	PUNCT
eurjchem-1251	304	1	m.p	m.p	PROPN
eurjchem-1251	304	2	.	.	PROPN
eurjchem-1251	304	3	:	:	PUNCT
eurjchem-1251	305	1	208‐210	208‐210	NUM
eurjchem-1251	305	2	°	°	ADP
eurjchem-1251	305	3	c	c	X
eurjchem-1251	305	4	.	.	PUNCT
eurjchem-1251	306	1	ft‐ir	ft‐ir	NOUN
eurjchem-1251	306	2	(	(	PUNCT
eurjchem-1251	306	3	kbr	kbr	PROPN
eurjchem-1251	306	4	,	,	PUNCT
eurjchem-1251	306	5	ν	ν	PROPN
eurjchem-1251	306	6	,	,	PUNCT
eurjchem-1251	306	7	cm‐1	cm‐1	PROPN
eurjchem-1251	306	8	):	):	PUNCT
eurjchem-1251	306	9	3389	3389	NUM
eurjchem-1251	306	10	,	,	PUNCT
eurjchem-1251	306	11	3342	3342	NUM
eurjchem-1251	306	12	(	(	PUNCT
eurjchem-1251	306	13	2nh	2nh	NOUN
eurjchem-1251	306	14	)	)	PUNCT
eurjchem-1251	306	15	,	,	PUNCT
eurjchem-1251	306	16	3061	3061	NUM
eurjchem-1251	306	17	(	(	PUNCT
eurjchem-1251	306	18	ch	ch	NOUN
eurjchem-1251	306	19	arom	arom	NOUN
eurjchem-1251	306	20	.	.	PUNCT
eurjchem-1251	306	21	)	)	PUNCT
eurjchem-1251	306	22	,	,	PUNCT
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eurjchem-1251	306	24	(	(	PUNCT
eurjchem-1251	306	25	no2	no2	PROPN
eurjchem-1251	306	26	asym	asym	PROPN
eurjchem-1251	306	27	.	.	PROPN
eurjchem-1251	306	28	)	)	PUNCT
eurjchem-1251	306	29	,	,	PUNCT
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eurjchem-1251	306	31	(	(	PUNCT
eurjchem-1251	306	32	no2	no2	PROPN
eurjchem-1251	306	33	sym	sym	PROPN
eurjchem-1251	306	34	.	.	PROPN
eurjchem-1251	306	35	)	)	PUNCT
eurjchem-1251	306	36	,	,	PUNCT
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eurjchem-1251	306	38	(	(	PUNCT
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eurjchem-1251	306	40	asym	asym	PROPN
eurjchem-1251	306	41	.	.	PROPN
eurjchem-1251	306	42	)	)	PUNCT
eurjchem-1251	306	43	,	,	PUNCT
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eurjchem-1251	306	45	(	(	PUNCT
eurjchem-1251	306	46	so2	so2	PROPN
eurjchem-1251	306	47	sym	sym	PROPN
eurjchem-1251	306	48	.	.	PUNCT
eurjchem-1251	306	49	)	)	PUNCT
eurjchem-1251	306	50	.	.	PUNCT
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eurjchem-1251	307	3	(	(	PUNCT
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eurjchem-1251	307	5	mhz	mhz	NOUN
eurjchem-1251	307	6	,	,	PUNCT
eurjchem-1251	307	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1251	307	8	,	,	PUNCT
eurjchem-1251	307	9	δ	δ	PROPN
eurjchem-1251	307	10	,	,	PUNCT
eurjchem-1251	307	11	ppm	ppm	NOUN
eurjchem-1251	307	12	):	):	PUNCT
eurjchem-1251	307	13	6.05	6.05	NUM
eurjchem-1251	307	14	(	(	PUNCT
eurjchem-1251	307	15	s	s	PROPN
eurjchem-1251	307	16	,	,	PUNCT
eurjchem-1251	307	17	1h	1h	NUM
eurjchem-1251	307	18	,	,	PUNCT
eurjchem-1251	307	19	nh	nh	PROPN
eurjchem-1251	307	20	)	)	PUNCT
eurjchem-1251	307	21	,	,	PUNCT
eurjchem-1251	307	22	6.53‐6.92	6.53‐6.92	NUM
eurjchem-1251	307	23	(	(	PUNCT
eurjchem-1251	307	24	m	m	PROPN
eurjchem-1251	307	25	,	,	PUNCT
eurjchem-1251	307	26	23h	23h	NOUN
eurjchem-1251	307	27	,	,	PUNCT
eurjchem-1251	307	28	ar‐h	ar‐h	PROPN
eurjchem-1251	307	29	)	)	PUNCT
eurjchem-1251	307	30	,	,	PUNCT
eurjchem-1251	307	31	10.49	10.49	NUM
eurjchem-1251	307	32	(	(	PUNCT
eurjchem-1251	307	33	s	s	PROPN
eurjchem-1251	307	34	,	,	PUNCT
eurjchem-1251	307	35	1h	1h	NUM
eurjchem-1251	307	36	,	,	PUNCT
eurjchem-1251	307	37	nhso2	nhso2	NOUN
eurjchem-1251	307	38	)	)	PUNCT
eurjchem-1251	307	39	.	.	PUNCT
eurjchem-1251	308	1	ms	ms	NOUN
eurjchem-1251	308	2	(	(	PUNCT
eurjchem-1251	308	3	ei	ei	PROPN
eurjchem-1251	308	4	,	,	PUNCT
eurjchem-1251	308	5	m	m	PROPN
eurjchem-1251	308	6	/	/	SYM
eurjchem-1251	308	7	z	z	PROPN
eurjchem-1251	308	8	(	(	PUNCT
eurjchem-1251	308	9	%	%	NOUN
eurjchem-1251	308	10	)	)	PUNCT
eurjchem-1251	308	11	):	):	PUNCT
eurjchem-1251	308	12	599	599	NUM
eurjchem-1251	308	13	(	(	PUNCT
eurjchem-1251	308	14	m+	m+	NUM
eurjchem-1251	308	15	,	,	PUNCT
eurjchem-1251	308	16	16.40	16.40	NUM
eurjchem-1251	308	17	)	)	PUNCT
eurjchem-1251	308	18	,	,	PUNCT
eurjchem-1251	308	19	554	554	NUM
eurjchem-1251	308	20	(	(	PUNCT
eurjchem-1251	308	21	8.84	8.84	NUM
eurjchem-1251	308	22	)	)	PUNCT
eurjchem-1251	308	23	,	,	PUNCT
eurjchem-1251	308	24	479	479	NUM
eurjchem-1251	308	25	(	(	PUNCT
eurjchem-1251	308	26	10.13	10.13	NUM
eurjchem-1251	308	27	)	)	PUNCT
eurjchem-1251	308	28	,	,	PUNCT
eurjchem-1251	308	29	422	422	NUM
eurjchem-1251	308	30	(	(	PUNCT
eurjchem-1251	308	31	11.25	11.25	NUM
eurjchem-1251	308	32	)	)	PUNCT
eurjchem-1251	308	33	,	,	PUNCT
eurjchem-1251	308	34	407	407	NUM
eurjchem-1251	308	35	(	(	PUNCT
eurjchem-1251	308	36	4.02	4.02	NUM
eurjchem-1251	308	37	)	)	PUNCT
eurjchem-1251	308	38	,	,	PUNCT
eurjchem-1251	308	39	395	395	NUM
eurjchem-1251	308	40	(	(	PUNCT
eurjchem-1251	308	41	9.97	9.97	NUM
eurjchem-1251	308	42	)	)	PUNCT
eurjchem-1251	308	43	,	,	PUNCT
eurjchem-1251	308	44	371	371	NUM
eurjchem-1251	308	45	(	(	PUNCT
eurjchem-1251	308	46	8.84	8.84	NUM
eurjchem-1251	308	47	)	)	PUNCT
eurjchem-1251	308	48	,	,	PUNCT
eurjchem-1251	308	49	323	323	NUM
eurjchem-1251	308	50	(	(	PUNCT
eurjchem-1251	308	51	4.82	4.82	NUM
eurjchem-1251	308	52	)	)	PUNCT
eurjchem-1251	308	53	,	,	PUNCT
eurjchem-1251	308	54	293	293	NUM
eurjchem-1251	308	55	(	(	PUNCT
eurjchem-1251	308	56	27.33	27.33	NUM
eurjchem-1251	308	57	)	)	PUNCT
eurjchem-1251	308	58	,	,	PUNCT
eurjchem-1251	308	59	277	277	NUM
eurjchem-1251	308	60	(	(	PUNCT
eurjchem-1251	308	61	18.17	18.17	NUM
eurjchem-1251	308	62	)	)	PUNCT
eurjchem-1251	308	63	,	,	PUNCT
eurjchem-1251	308	64	206	206	NUM
eurjchem-1251	308	65	(	(	PUNCT
eurjchem-1251	308	66	10.61	10.61	NUM
eurjchem-1251	308	67	)	)	PUNCT
eurjchem-1251	308	68	,	,	PUNCT
eurjchem-1251	308	69	202	202	NUM
eurjchem-1251	308	70	(	(	PUNCT
eurjchem-1251	308	71	2.73	2.73	NUM
eurjchem-1251	308	72	)	)	PUNCT
eurjchem-1251	308	73	,	,	PUNCT
eurjchem-1251	308	74	191	191	NUM
eurjchem-1251	308	75	(	(	PUNCT
eurjchem-1251	308	76	8.36	8.36	NUM
eurjchem-1251	308	77	)	)	PUNCT
eurjchem-1251	308	78	,	,	PUNCT
eurjchem-1251	308	79	178	178	NUM
eurjchem-1251	308	80	(	(	PUNCT
eurjchem-1251	308	81	7.72	7.72	NUM
eurjchem-1251	308	82	)	)	PUNCT
eurjchem-1251	308	83	,	,	PUNCT
eurjchem-1251	308	84	138	138	NUM
eurjchem-1251	308	85	(	(	PUNCT
eurjchem-1251	308	86	38.26	38.26	NUM
eurjchem-1251	308	87	)	)	PUNCT
eurjchem-1251	308	88	,	,	PUNCT
eurjchem-1251	308	89	92	92	NUM
eurjchem-1251	308	90	(	(	PUNCT
eurjchem-1251	308	91	100	100	NUM
eurjchem-1251	308	92	)	)	PUNCT
eurjchem-1251	308	93	.	.	PUNCT
eurjchem-1251	309	1	anal	anal	PROPN
eurjchem-1251	309	2	.	.	PUNCT
eurjchem-1251	309	3	calcd	calcd	NOUN
eurjchem-1251	309	4	.	.	PUNCT
eurjchem-1251	310	1	for	for	ADP
eurjchem-1251	310	2	c34h25n5o4s	c34h25n5o4s	NUM
eurjchem-1251	310	3	:	:	PUNCT
eurjchem-1251	310	4	c	c	X
eurjchem-1251	310	5	,	,	PUNCT
eurjchem-1251	310	6	68.10	68.10	NUM
eurjchem-1251	310	7	;	;	PUNCT
eurjchem-1251	310	8	h	h	X
eurjchem-1251	310	9	,	,	PUNCT
eurjchem-1251	310	10	4.20	4.20	NUM
eurjchem-1251	310	11	;	;	PUNCT
eurjchem-1251	310	12	n	n	CCONJ
eurjchem-1251	310	13	,	,	PUNCT
eurjchem-1251	310	14	11.68	11.68	NUM
eurjchem-1251	310	15	.	.	PUNCT
eurjchem-1251	310	16	found	find	VERB
eurjchem-1251	310	17	:	:	PUNCT
eurjchem-1251	311	1	c	c	X
eurjchem-1251	311	2	,	,	PUNCT
eurjchem-1251	311	3	68.40	68.40	NUM
eurjchem-1251	311	4	;	;	PUNCT
eurjchem-1251	312	1	h	h	NOUN
eurjchem-1251	312	2	,	,	PUNCT
eurjchem-1251	312	3	4.10	4.10	NUM
eurjchem-1251	312	4	;	;	PUNCT
eurjchem-1251	312	5	n	n	CCONJ
eurjchem-1251	312	6	,	,	PUNCT
eurjchem-1251	312	7	11.9	11.9	NUM
eurjchem-1251	312	8	%	%	NOUN
eurjchem-1251	312	9	.	.	PUNCT
eurjchem-1251	313	1	2.3	2.3	NUM
eurjchem-1251	313	2	.	.	PUNCT
eurjchem-1251	313	3	antimicrobial	antimicrobial	ADJ
eurjchem-1251	313	4	activity	activity	NOUN
eurjchem-1251	313	5	applying	apply	VERB
eurjchem-1251	313	6	the	the	DET
eurjchem-1251	313	7	agar	agar	NOUN
eurjchem-1251	313	8	plate	plate	NOUN
eurjchem-1251	313	9	diffusion	diffusion	NOUN
eurjchem-1251	313	10	technique	technique	NOUN
eurjchem-1251	313	11	[	[	X
eurjchem-1251	313	12	18	18	NUM
eurjchem-1251	313	13	]	]	PUNCT
eurjchem-1251	313	14	,	,	PUNCT
eurjchem-1251	313	15	the	the	DET
eurjchem-1251	313	16	newly	newly	ADV
eurjchem-1251	313	17	synthesised	synthesise	VERB
eurjchem-1251	313	18	compounds	compound	NOUN
eurjchem-1251	313	19	were	be	AUX
eurjchem-1251	313	20	screened	screen	VERB
eurjchem-1251	313	21	for	for	ADP
eurjchem-1251	313	22	their	their	PRON
eurjchem-1251	313	23	antimicrobial	antimicrobial	ADJ
eurjchem-1251	313	24	activity	activity	NOUN
eurjchem-1251	313	25	against	against	ADP
eurjchem-1251	313	26	some	some	DET
eurjchem-1251	313	27	gram	gram	NOUN
eurjchem-1251	313	28	positive	positive	ADJ
eurjchem-1251	313	29	bacteria	bacteria	NOUN
eurjchem-1251	313	30	(	(	PUNCT
eurjchem-1251	313	31	staphylococcus	staphylococcus	NOUN
eurjchem-1251	313	32	aureus	aureus	NOUN
eurjchem-1251	313	33	and	and	CCONJ
eurjchem-1251	313	34	bacillus	bacillus	NOUN
eurjchem-1251	313	35	subtilis	subtili	NOUN
eurjchem-1251	313	36	)	)	PUNCT
eurjchem-1251	313	37	,	,	PUNCT
eurjchem-1251	313	38	gram	gram	PROPN
eurjchem-1251	313	39	negative	negative	ADJ
eurjchem-1251	313	40	bacteria	bacteria	NOUN
eurjchem-1251	313	41	(	(	PUNCT
eurjchem-1251	313	42	escherichia	escherichia	NOUN
eurjchem-1251	313	43	coli	coli	NOUN
eurjchem-1251	313	44	and	and	CCONJ
eurjchem-1251	313	45	pseudomonas	pseudomona	NOUN
eurjchem-1251	313	46	aeruginosa	aeruginosa	NOUN
eurjchem-1251	313	47	)	)	PUNCT
eurjchem-1251	313	48	,	,	PUNCT
eurjchem-1251	313	49	yeast	yeast	NOUN
eurjchem-1251	313	50	(	(	PUNCT
eurjchem-1251	313	51	candida	candida	NOUN
eurjchem-1251	313	52	albicans	albican	NOUN
eurjchem-1251	313	53	)	)	PUNCT
eurjchem-1251	313	54	,	,	PUNCT
eurjchem-1251	313	55	and	and	CCONJ
eurjchem-1251	313	56	fungi	fungus	NOUN
eurjchem-1251	313	57	(	(	PUNCT
eurjchem-1251	313	58	aspergillus	aspergillus	NOUN
eurjchem-1251	313	59	niger	niger	NOUN
eurjchem-1251	313	60	)	)	PUNCT
eurjchem-1251	313	61	.	.	PUNCT
eurjchem-1251	314	1	in	in	ADP
eurjchem-1251	314	2	this	this	DET
eurjchem-1251	314	3	method	method	NOUN
eurjchem-1251	314	4	,	,	PUNCT
eurjchem-1251	314	5	a	a	DET
eurjchem-1251	314	6	standard	standard	ADJ
eurjchem-1251	314	7	5	5	NUM
eurjchem-1251	314	8	mm	mm	NOUN
eurjchem-1251	314	9	sterilised	sterilise	VERB
eurjchem-1251	314	10	filter	filter	NOUN
eurjchem-1251	314	11	paper	paper	NOUN
eurjchem-1251	314	12	disk	disk	NOUN
eurjchem-1251	314	13	impregnated	impregnate	VERB
eurjchem-1251	314	14	with	with	ADP
eurjchem-1251	314	15	the	the	DET
eurjchem-1251	314	16	compound	compound	NOUN
eurjchem-1251	314	17	(	(	PUNCT
eurjchem-1251	314	18	0.3	0.3	NUM
eurjchem-1251	314	19	mg	mg	NOUN
eurjchem-1251	314	20	in	in	ADP
eurjchem-1251	314	21	0.1	0.1	NUM
eurjchem-1251	314	22	ml	ml	NOUN
eurjchem-1251	314	23	of	of	ADP
eurjchem-1251	314	24	dimethylformamide	dimethylformamide	NOUN
eurjchem-1251	314	25	)	)	PUNCT
eurjchem-1251	314	26	was	be	AUX
eurjchem-1251	314	27	placed	place	VERB
eurjchem-1251	314	28	on	on	ADP
eurjchem-1251	314	29	agar	agar	NOUN
eurjchem-1251	314	30	plate	plate	NOUN
eurjchem-1251	314	31	seeded	seed	VERB
eurjchem-1251	314	32	with	with	ADP
eurjchem-1251	314	33	the	the	DET
eurjchem-1251	314	34	tested	test	VERB
eurjchem-1251	314	35	organism	organism	NOUN
eurjchem-1251	314	36	.	.	PUNCT
eurjchem-1251	315	1	the	the	DET
eurjchem-1251	315	2	plates	plate	NOUN
eurjchem-1251	315	3	were	be	AUX
eurjchem-1251	315	4	incubated	incubate	VERB
eurjchem-1251	315	5	for	for	ADP
eurjchem-1251	315	6	24	24	NUM
eurjchem-1251	315	7	h	h	NOUN
eurjchem-1251	315	8	at	at	ADP
eurjchem-1251	315	9	37	37	NUM
eurjchem-1251	315	10	°	°	ADP
eurjchem-1251	315	11	c	c	NOUN
eurjchem-1251	315	12	for	for	ADP
eurjchem-1251	315	13	bacteria	bacteria	NOUN
eurjchem-1251	315	14	,	,	PUNCT
eurjchem-1251	315	15	and	and	CCONJ
eurjchem-1251	315	16	for	for	ADP
eurjchem-1251	315	17	four	four	NUM
eurjchem-1251	315	18	days	day	NOUN
eurjchem-1251	315	19	at	at	ADP
eurjchem-1251	315	20	28	28	NUM
eurjchem-1251	315	21	°	°	ADP
eurjchem-1251	315	22	c	c	PROPN
eurjchem-1251	315	23	for	for	ADP
eurjchem-1251	315	24	fungi	fungi	PROPN
eurjchem-1251	315	25	.	.	PUNCT
eurjchem-1251	316	1	the	the	DET
eurjchem-1251	316	2	inhibition	inhibition	NOUN
eurjchem-1251	316	3	zone	zone	NOUN
eurjchem-1251	316	4	of	of	ADP
eurjchem-1251	316	5	bacteria	bacteria	NOUN
eurjchem-1251	316	6	and	and	CCONJ
eurjchem-1251	316	7	fungi	fungus	NOUN
eurjchem-1251	316	8	growth	growth	NOUN
eurjchem-1251	316	9	around	around	ADP
eurjchem-1251	316	10	the	the	DET
eurjchem-1251	316	11	disk	disk	NOUN
eurjchem-1251	316	12	were	be	AUX
eurjchem-1251	316	13	determined	determine	VERB
eurjchem-1251	316	14	.	.	PUNCT
eurjchem-1251	317	1	3	3	X
eurjchem-1251	317	2	.	.	NOUN
eurjchem-1251	317	3	results	result	NOUN
eurjchem-1251	317	4	and	and	CCONJ
eurjchem-1251	317	5	discussion	discussion	NOUN
eurjchem-1251	317	6	3.1	3.1	NUM
eurjchem-1251	317	7	.	.	PUNCT
eurjchem-1251	318	1	synthesis	synthesis	NOUN
eurjchem-1251	318	2	during	during	ADP
eurjchem-1251	318	3	a	a	DET
eurjchem-1251	318	4	study	study	NOUN
eurjchem-1251	318	5	of	of	ADP
eurjchem-1251	318	6	the	the	DET
eurjchem-1251	318	7	synthesis	synthesis	NOUN
eurjchem-1251	318	8	of	of	ADP
eurjchem-1251	318	9	pyridazine	pyridazine	NOUN
eurjchem-1251	318	10	derivatives	derivative	NOUN
eurjchem-1251	318	11	,	,	PUNCT
eurjchem-1251	318	12	3‐aminopyridazine	3‐aminopyridazine	NUM
eurjchem-1251	318	13	(	(	PUNCT
eurjchem-1251	318	14	5	5	NUM
eurjchem-1251	318	15	)	)	PUNCT
eurjchem-1251	318	16	was	be	AUX
eurjchem-1251	318	17	selected	select	VERB
eurjchem-1251	318	18	as	as	ADP
eurjchem-1251	318	19	an	an	DET
eurjchem-1251	318	20	ideal	ideal	ADJ
eurjchem-1251	318	21	starting	starting	NOUN
eurjchem-1251	318	22	material	material	NOUN
eurjchem-1251	318	23	for	for	ADP
eurjchem-1251	318	24	our	our	PRON
eurjchem-1251	318	25	purpose	purpose	NOUN
eurjchem-1251	318	26	.	.	PUNCT
eurjchem-1251	319	1	its	its	PRON
eurjchem-1251	319	2	preparation	preparation	NOUN
eurjchem-1251	319	3	was	be	AUX
eurjchem-1251	319	4	accomplished	accomplish	VERB
eurjchem-1251	319	5	via	via	ADP
eurjchem-1251	319	6	the	the	DET
eurjchem-1251	319	7	classical	classical	ADJ
eurjchem-1251	319	8	staudinger	staudinger	NOUN
eurjchem-1251	319	9	reaction	reaction	NOUN
eurjchem-1251	319	10	[	[	X
eurjchem-1251	319	11	17	17	NUM
eurjchem-1251	319	12	]	]	PUNCT
eurjchem-1251	319	13	.	.	PUNCT
eurjchem-1251	320	1	tetrazolopyridazine	tetrazolopyridazine	NOUN
eurjchem-1251	320	2	(	(	PUNCT
eurjchem-1251	320	3	3	3	X
eurjchem-1251	320	4	)	)	PUNCT
eurjchem-1251	320	5	was	be	AUX
eurjchem-1251	320	6	reduced	reduce	VERB
eurjchem-1251	320	7	to	to	ADP
eurjchem-1251	320	8	the	the	DET
eurjchem-1251	320	9	corresponding	correspond	VERB
eurjchem-1251	320	10	aminopyridazine	aminopyridazine	NOUN
eurjchem-1251	320	11	5	5	NUM
eurjchem-1251	320	12	via	via	ADP
eurjchem-1251	320	13	formation	formation	NOUN
eurjchem-1251	320	14	of	of	ADP
eurjchem-1251	320	15	phosphazene	phosphazene	NOUN
eurjchem-1251	320	16	intermediate	intermediate	ADJ
eurjchem-1251	320	17	(	(	PUNCT
eurjchem-1251	320	18	4	4	NUM
eurjchem-1251	320	19	)	)	PUNCT
eurjchem-1251	320	20	,	,	PUNCT
eurjchem-1251	320	21	as	as	SCONJ
eurjchem-1251	320	22	depicted	depict	VERB
eurjchem-1251	320	23	in	in	ADP
eurjchem-1251	320	24	(	(	PUNCT
eurjchem-1251	320	25	scheme	scheme	NOUN
eurjchem-1251	320	26	1	1	NUM
eurjchem-1251	320	27	)	)	PUNCT
eurjchem-1251	320	28	.	.	PUNCT
eurjchem-1251	321	1	3‐chloro‐4	3‐chloro‐4	NUM
eurjchem-1251	321	2	,	,	PUNCT
eurjchem-1251	321	3	5	5	NUM
eurjchem-1251	321	4	,	,	PUNCT
eurjchem-1251	321	5	6‐triphenylpyridazine	6‐triphenylpyridazine	NUM
eurjchem-1251	321	6	(	(	PUNCT
eurjchem-1251	321	7	2	2	NUM
eurjchem-1251	321	8	)	)	PUNCT
eurjchem-1251	321	9	was	be	AUX
eurjchem-1251	321	10	obtained	obtain	VERB
eurjchem-1251	321	11	by	by	ADP
eurjchem-1251	321	12	treatment	treatment	NOUN
eurjchem-1251	321	13	of	of	ADP
eurjchem-1251	321	14	4,5,6‐triphenylpyridazin‐3(2h)‐	4,5,6‐triphenylpyridazin‐3(2h)‐	NUM
eurjchem-1251	321	15	one(1	one(1	NOUN
eurjchem-1251	321	16	)	)	PUNCT
eurjchem-1251	321	17	with	with	ADP
eurjchem-1251	321	18	phosphoryl	phosphoryl	PROPN
eurjchem-1251	321	19	chloride	chloride	PROPN
eurjchem-1251	321	20	at	at	ADP
eurjchem-1251	321	21	refluxing	refluxing	NOUN
eurjchem-1251	321	22	temperature	temperature	NOUN
eurjchem-1251	321	23	.	.	PUNCT
eurjchem-1251	322	1	azidation	azidation	NOUN
eurjchem-1251	322	2	of	of	ADP
eurjchem-1251	322	3	compound	compound	NOUN
eurjchem-1251	322	4	2	2	NUM
eurjchem-1251	322	5	with	with	ADP
eurjchem-1251	322	6	sodium	sodium	NOUN
eurjchem-1251	322	7	azide	azide	NOUN
eurjchem-1251	322	8	in	in	ADP
eurjchem-1251	322	9	dimethyl	dimethyl	NOUN
eurjchem-1251	322	10	formamide	formamide	ADV
eurjchem-1251	322	11	at	at	ADP
eurjchem-1251	322	12	100	100	NUM
eurjchem-1251	322	13	°	°	NOUN
eurjchem-1251	322	14	c	c	NOUN
eurjchem-1251	322	15	gave	give	VERB
eurjchem-1251	322	16	the	the	DET
eurjchem-1251	322	17	corresponding	corresponding	ADJ
eurjchem-1251	322	18	tetrazolo[1,5‐	tetrazolo[1,5‐	PROPN
eurjchem-1251	322	19	b]pyridazine	b]pyridazine	PROPN
eurjchem-1251	322	20	,	,	PUNCT
eurjchem-1251	322	21	3	3	NUM
eurjchem-1251	322	22	[	[	X
eurjchem-1251	322	23	15,16	15,16	NUM
eurjchem-1251	322	24	]	]	PUNCT
eurjchem-1251	322	25	.	.	PUNCT
eurjchem-1251	323	1	refluxing	refluxe	VERB
eurjchem-1251	323	2	the	the	DET
eurjchem-1251	323	3	latter	latter	ADJ
eurjchem-1251	323	4	compound	compound	NOUN
eurjchem-1251	323	5	with	with	ADP
eurjchem-1251	323	6	one	one	NUM
eurjchem-1251	323	7	equivalent	equivalent	NOUN
eurjchem-1251	323	8	of	of	ADP
eurjchem-1251	323	9	triphenylphosphine	triphenylphosphine	NOUN
eurjchem-1251	323	10	in	in	ADP
eurjchem-1251	323	11	1,2‐dichlorobenzene	1,2‐dichlorobenzene	NOUN
eurjchem-1251	323	12	for	for	ADP
eurjchem-1251	323	13	3	3	NUM
eurjchem-1251	323	14	hours	hour	NOUN
eurjchem-1251	323	15	yielded	yield	VERB
eurjchem-1251	323	16	4,5,6‐triphenyl‐n‐(triphenylphosphanyli‐	4,5,6‐triphenyl‐n‐(triphenylphosphanyli‐	NUM
eurjchem-1251	323	17	dene)pyridazin‐3‐amine	dene)pyridazin‐3‐amine	NOUN
eurjchem-1251	323	18	(	(	PUNCT
eurjchem-1251	323	19	4	4	NUM
eurjchem-1251	323	20	)	)	PUNCT
eurjchem-1251	324	1	[	[	X
eurjchem-1251	324	2	17	17	NUM
eurjchem-1251	324	3	]	]	PUNCT
eurjchem-1251	324	4	.	.	PUNCT
eurjchem-1251	325	1	subsequent	subsequent	ADJ
eurjchem-1251	325	2	acid	acid	NOUN
eurjchem-1251	325	3	hydrolysis	hydrolysis	NOUN
eurjchem-1251	325	4	of	of	ADP
eurjchem-1251	325	5	compound	compound	NOUN
eurjchem-1251	325	6	4	4	NUM
eurjchem-1251	325	7	with	with	ADP
eurjchem-1251	325	8	a	a	DET
eurjchem-1251	325	9	mixture	mixture	NOUN
eurjchem-1251	325	10	of	of	ADP
eurjchem-1251	325	11	acetic	acetic	ADJ
eurjchem-1251	325	12	acid	acid	NOUN
eurjchem-1251	325	13	:	:	PUNCT
eurjchem-1251	325	14	water	water	NOUN
eurjchem-1251	325	15	(	(	PUNCT
eurjchem-1251	325	16	4:1	4:1	NUM
eurjchem-1251	325	17	,	,	PUNCT
eurjchem-1251	325	18	v	v	NOUN
eurjchem-1251	325	19	:	:	PUNCT
eurjchem-1251	325	20	v	v	NOUN
eurjchem-1251	325	21	)	)	PUNCT
eurjchem-1251	325	22	provided	provide	VERB
eurjchem-1251	325	23	the	the	DET
eurjchem-1251	325	24	corresponding	correspond	VERB
eurjchem-1251	325	25	3‐aminopyridazine	3‐aminopyridazine	NUM
eurjchem-1251	325	26	intermediate	intermediate	ADJ
eurjchem-1251	325	27	5	5	NUM
eurjchem-1251	325	28	,	,	PUNCT
eurjchem-1251	325	29	in	in	ADP
eurjchem-1251	325	30	86	86	NUM
eurjchem-1251	325	31	%	%	NOUN
eurjchem-1251	325	32	yield	yield	NOUN
eurjchem-1251	325	33	.	.	PUNCT
eurjchem-1251	326	1	the	the	DET
eurjchem-1251	326	2	structure	structure	NOUN
eurjchem-1251	326	3	of	of	ADP
eurjchem-1251	326	4	compound	compound	NOUN
eurjchem-1251	326	5	5	5	NUM
eurjchem-1251	326	6	was	be	AUX
eurjchem-1251	326	7	established	establish	VERB
eurjchem-1251	326	8	by	by	ADP
eurjchem-1251	326	9	the	the	DET
eurjchem-1251	326	10	presence	presence	NOUN
eurjchem-1251	326	11	of	of	ADP
eurjchem-1251	326	12	stretching	stretch	VERB
eurjchem-1251	326	13	absorption	absorption	NOUN
eurjchem-1251	326	14	bands	band	NOUN
eurjchem-1251	326	15	at	at	ADP
eurjchem-1251	326	16	3473	3473	NUM
eurjchem-1251	326	17	and	and	CCONJ
eurjchem-1251	326	18	3280	3280	NUM
eurjchem-1251	326	19	cm‐1	cm‐1	NOUN
eurjchem-1251	326	20	in	in	ADP
eurjchem-1251	326	21	the	the	DET
eurjchem-1251	326	22	ir	ir	PROPN
eurjchem-1251	326	23	spectrum	spectrum	NOUN
eurjchem-1251	326	24	due	due	ADP
eurjchem-1251	326	25	to	to	ADP
eurjchem-1251	326	26	nh2	nh2	PROPN
eurjchem-1251	326	27	group	group	NOUN
eurjchem-1251	326	28	.	.	PUNCT
eurjchem-1251	327	1	it	it	PRON
eurjchem-1251	327	2	was	be	AUX
eurjchem-1251	327	3	also	also	ADV
eurjchem-1251	327	4	supported	support	VERB
eurjchem-1251	327	5	by	by	ADP
eurjchem-1251	327	6	the	the	DET
eurjchem-1251	327	7	presence	presence	NOUN
eurjchem-1251	327	8	of	of	ADP
eurjchem-1251	327	9	d2o	d2o	PROPN
eurjchem-1251	327	10	exchangeable	exchangeable	ADJ
eurjchem-1251	327	11	broad	broad	ADJ
eurjchem-1251	327	12	singlet	singlet	ADJ
eurjchem-1251	327	13	band	band	NOUN
eurjchem-1251	327	14	due	due	ADP
eurjchem-1251	327	15	to	to	ADP
eurjchem-1251	327	16	the	the	DET
eurjchem-1251	327	17	nh2	nh2	NOUN
eurjchem-1251	327	18	protons	proton	NOUN
eurjchem-1251	327	19	at	at	ADP
eurjchem-1251	327	20	5.80	5.80	NUM
eurjchem-1251	327	21	ppm	ppm	NOUN
eurjchem-1251	327	22	in	in	ADP
eurjchem-1251	327	23	1h	1h	NUM
eurjchem-1251	327	24	nmr	nmr	NOUN
eurjchem-1251	327	25	.	.	PUNCT
eurjchem-1251	328	1	in	in	ADP
eurjchem-1251	328	2	addition	addition	NOUN
eurjchem-1251	328	3	,	,	PUNCT
eurjchem-1251	328	4	the	the	DET
eurjchem-1251	328	5	mass	mass	NOUN
eurjchem-1251	328	6	spectrum	spectrum	NOUN
eurjchem-1251	328	7	showed	show	VERB
eurjchem-1251	328	8	the	the	DET
eurjchem-1251	328	9	molecular	molecular	ADJ
eurjchem-1251	328	10	ion	ion	NOUN
eurjchem-1251	328	11	peak	peak	NOUN
eurjchem-1251	328	12	m+	m+	NUM
eurjchem-1251	328	13	at	at	ADP
eurjchem-1251	328	14	m	m	PROPN
eurjchem-1251	328	15	/	/	SYM
eurjchem-1251	328	16	z	z	PROPN
eurjchem-1251	328	17	=	=	SYM
eurjchem-1251	328	18	323	323	NUM
eurjchem-1251	328	19	,	,	PUNCT
eurjchem-1251	328	20	which	which	PRON
eurjchem-1251	328	21	was	be	AUX
eurjchem-1251	328	22	in	in	ADP
eurjchem-1251	328	23	agreement	agreement	NOUN
eurjchem-1251	328	24	with	with	ADP
eurjchem-1251	328	25	the	the	DET
eurjchem-1251	328	26	calculated	calculate	VERB
eurjchem-1251	328	27	molecular	molecular	ADJ
eurjchem-1251	328	28	weight	weight	NOUN
eurjchem-1251	328	29	(	(	PUNCT
eurjchem-1251	328	30	c22h17n3).treatment	c22h17n3).treatment	NOUN
eurjchem-1251	328	31	of	of	ADP
eurjchem-1251	328	32	compound	compound	NOUN
eurjchem-1251	328	33	5with	5with	NUM
eurjchem-1251	328	34	hydrochloric	hydrochloric	ADJ
eurjchem-1251	328	35	acid	acid	NOUN
eurjchem-1251	328	36	/	/	SYM
eurjchem-1251	328	37	sodium	sodium	NOUN
eurjchem-1251	328	38	nitrite	nitrite	NOUN
eurjchem-1251	328	39	solution	solution	NOUN
eurjchem-1251	328	40	,	,	PUNCT
eurjchem-1251	328	41	carried	carry	VERB
eurjchem-1251	328	42	out	out	ADP
eurjchem-1251	328	43	at	at	ADP
eurjchem-1251	328	44	low	low	ADJ
eurjchem-1251	328	45	temperature	temperature	NOUN
eurjchem-1251	328	46	,	,	PUNCT
eurjchem-1251	328	47	gave	give	VERB
eurjchem-1251	328	48	a	a	DET
eurjchem-1251	328	49	single	single	ADJ
eurjchem-1251	328	50	product	product	NOUN
eurjchem-1251	328	51	obtained	obtain	VERB
eurjchem-1251	328	52	from	from	ADP
eurjchem-1251	328	53	the	the	DET
eurjchem-1251	328	54	diazonium	diazonium	NOUN
eurjchem-1251	328	55	ion	ion	NOUN
eurjchem-1251	328	56	,	,	PUNCT
eurjchem-1251	328	57	which	which	PRON
eurjchem-1251	328	58	was	be	AUX
eurjchem-1251	328	59	generated	generate	VERB
eurjchem-1251	328	60	as	as	ADP
eurjchem-1251	328	61	an	an	DET
eurjchem-1251	328	62	intermediate	intermediate	NOUN
eurjchem-1251	328	63	followed	follow	VERB
eurjchem-1251	328	64	by	by	ADP
eurjchem-1251	328	65	ultimate	ultimate	ADJ
eurjchem-1251	328	66	hydroxylation	hydroxylation	NOUN
eurjchem-1251	328	67	.	.	PUNCT
eurjchem-1251	329	1	the	the	DET
eurjchem-1251	329	2	isolated	isolated	ADJ
eurjchem-1251	329	3	product	product	NOUN
eurjchem-1251	329	4	was	be	AUX
eurjchem-1251	329	5	found	find	VERB
eurjchem-1251	329	6	to	to	PART
eurjchem-1251	329	7	be	be	AUX
eurjchem-1251	329	8	identical	identical	ADJ
eurjchem-1251	329	9	with	with	ADP
eurjchem-1251	329	10	the	the	DET
eurjchem-1251	329	11	authentic	authentic	ADJ
eurjchem-1251	329	12	sample	sample	NOUN
eurjchem-1251	329	13	1	1	NUM
eurjchem-1251	329	14	(	(	PUNCT
eurjchem-1251	329	15	m.p	m.p	PROPN
eurjchem-1251	329	16	.	.	PROPN
eurjchem-1251	329	17	,	,	PUNCT
eurjchem-1251	329	18	mixed	mixed	ADJ
eurjchem-1251	329	19	m.p	m.p	PROPN
eurjchem-1251	329	20	.	.	PROPN
eurjchem-1251	329	21	and	and	CCONJ
eurjchem-1251	329	22	identical	identical	ADJ
eurjchem-1251	329	23	ir	ir	PROPN
eurjchem-1251	329	24	spectra	spectra	PROPN
eurjchem-1251	329	25	)	)	PUNCT
eurjchem-1251	329	26	,	,	PUNCT
eurjchem-1251	329	27	which	which	PRON
eurjchem-1251	329	28	was	be	AUX
eurjchem-1251	329	29	synthesized	synthesize	VERB
eurjchem-1251	329	30	according	accord	VERB
eurjchem-1251	329	31	to	to	PART
eurjchem-1251	329	32	method	method	VERB
eurjchem-1251	329	33	a	a	DET
eurjchem-1251	329	34	[	[	X
eurjchem-1251	329	35	14	14	NUM
eurjchem-1251	329	36	]	]	PUNCT
eurjchem-1251	329	37	(	(	PUNCT
eurjchem-1251	329	38	scheme	scheme	NOUN
eurjchem-1251	329	39	1	1	NUM
eurjchem-1251	329	40	)	)	PUNCT
eurjchem-1251	329	41	.	.	PUNCT
eurjchem-1251	330	1	formylation	formylation	NOUN
eurjchem-1251	330	2	,	,	PUNCT
eurjchem-1251	330	3	acetylation	acetylation	NOUN
eurjchem-1251	330	4	,	,	PUNCT
eurjchem-1251	330	5	and	and	CCONJ
eurjchem-1251	330	6	benzoylation	benzoylation	NOUN
eurjchem-1251	330	7	of	of	ADP
eurjchem-1251	330	8	the	the	DET
eurjchem-1251	330	9	amino	amino	NOUN
eurjchem-1251	330	10	group	group	NOUN
eurjchem-1251	330	11	in	in	ADP
eurjchem-1251	330	12	compound	compound	NOUN
eurjchem-1251	330	13	5	5	NUM
eurjchem-1251	330	14	were	be	AUX
eurjchem-1251	330	15	achieved	achieve	VERB
eurjchem-1251	330	16	successfully	successfully	ADV
eurjchem-1251	330	17	by	by	ADP
eurjchem-1251	330	18	heating	heat	VERB
eurjchem-1251	330	19	with	with	ADP
eurjchem-1251	330	20	formic	formic	PROPN
eurjchem-1251	330	21	acid/	acid/	NUM
eurjchem-1251	330	22	dimethylformamide	dimethylformamide	NOUN
eurjchem-1251	330	23	,	,	PUNCT
eurjchem-1251	330	24	acetic	acetic	ADJ
eurjchem-1251	330	25	anhydride	anhydride	NOUN
eurjchem-1251	330	26	,	,	PUNCT
eurjchem-1251	330	27	and	and	CCONJ
eurjchem-1251	330	28	benzoyl	benzoyl	NOUN
eurjchem-1251	330	29	chloride/	chloride/	NUM
eurjchem-1251	330	30	pyridine	pyridine	NOUN
eurjchem-1251	330	31	at	at	ADP
eurjchem-1251	330	32	refluxing	refluxing	NOUN
eurjchem-1251	330	33	temperature	temperature	NOUN
eurjchem-1251	330	34	to	to	PART
eurjchem-1251	330	35	afford	afford	VERB
eurjchem-1251	330	36	n‐(4,5,6‐triphenyl	n‐(4,5,6‐triphenyl	SYM
eurjchem-1251	330	37	pyridazin‐3‐yl)formamide	pyridazin‐3‐yl)formamide	NOUN
eurjchem-1251	330	38	6a	6a	NOUN
eurjchem-1251	330	39	,	,	PUNCT
eurjchem-1251	330	40	n‐(4,5,6‐triphenylpyridazin‐3‐	n‐(4,5,6‐triphenylpyridazin‐3‐	NUM
eurjchem-1251	330	41	yl)acetamide	yl)acetamide	NOUN
eurjchem-1251	330	42	6b	6b	NOUN
eurjchem-1251	330	43	and	and	CCONJ
eurjchem-1251	330	44	n‐(4,5,6‐triphenylpyridazin‐3‐yl)benza‐	n‐(4,5,6‐triphenylpyridazin‐3‐yl)benza‐	NUM
eurjchem-1251	330	45	mide	mide	NOUN
eurjchem-1251	330	46	6c	6c	PROPN
eurjchem-1251	330	47	,	,	PUNCT
eurjchem-1251	330	48	respectively	respectively	ADV
eurjchem-1251	330	49	.	.	PUNCT
eurjchem-1251	331	1	furthermore	furthermore	ADV
eurjchem-1251	331	2	,	,	PUNCT
eurjchem-1251	331	3	reaction	reaction	NOUN
eurjchem-1251	331	4	of	of	ADP
eurjchem-1251	331	5	compound	compound	NOUN
eurjchem-1251	331	6	5	5	NUM
eurjchem-1251	331	7	with	with	ADP
eurjchem-1251	331	8	chloroacetyl	chloroacetyl	PROPN
eurjchem-1251	331	9	chloride	chloride	NOUN
eurjchem-1251	331	10	in	in	ADP
eurjchem-1251	331	11	pyridine	pyridine	NOUN
eurjchem-1251	331	12	at	at	ADP
eurjchem-1251	331	13	room	room	NOUN
eurjchem-1251	331	14	temperature	temperature	NOUN
eurjchem-1251	331	15	yielded	yield	VERB
eurjchem-1251	331	16	2‐chloro‐n‐	2‐chloro‐n‐	NUM
eurjchem-1251	331	17	(	(	PUNCT
eurjchem-1251	331	18	4,5,6‐triphenylpyridazin‐3‐yl)acetamide	4,5,6‐triphenylpyridazin‐3‐yl)acetamide	NUM
eurjchem-1251	331	19	6d	6d	NUM
eurjchem-1251	331	20	(	(	PUNCT
eurjchem-1251	331	21	scheme	scheme	NOUN
eurjchem-1251	331	22	2	2	NUM
eurjchem-1251	331	23	)	)	PUNCT
eurjchem-1251	331	24	.	.	PUNCT
eurjchem-1251	332	1	the	the	DET
eurjchem-1251	332	2	structures	structure	NOUN
eurjchem-1251	332	3	of	of	ADP
eurjchem-1251	332	4	compounds	compound	NOUN
eurjchem-1251	332	5	6a‐d	6a‐d	PROPN
eurjchem-1251	332	6	were	be	AUX
eurjchem-1251	332	7	confirmed	confirm	VERB
eurjchem-1251	332	8	on	on	ADP
eurjchem-1251	332	9	the	the	DET
eurjchem-1251	332	10	basis	basis	NOUN
eurjchem-1251	332	11	of	of	ADP
eurjchem-1251	332	12	spectroscopic	spectroscopic	ADJ
eurjchem-1251	332	13	data	datum	NOUN
eurjchem-1251	332	14	(	(	PUNCT
eurjchem-1251	332	15	ir	ir	PROPN
eurjchem-1251	332	16	,	,	PUNCT
eurjchem-1251	332	17	mass	mass	PROPN
eurjchem-1251	332	18	,	,	PUNCT
eurjchem-1251	332	19	and1h	and1h	PROPN
eurjchem-1251	332	20	nmr	nmr	NOUN
eurjchem-1251	332	21	spectra	spectra	NOUN
eurjchem-1251	332	22	)	)	PUNCT
eurjchem-1251	332	23	and	and	CCONJ
eurjchem-1251	332	24	elemen‐	elemen‐	NOUN
eurjchem-1251	332	25	tal	tal	ADJ
eurjchem-1251	332	26	analysis	analysis	NOUN
eurjchem-1251	332	27	as	as	SCONJ
eurjchem-1251	332	28	described	describe	VERB
eurjchem-1251	332	29	in	in	ADP
eurjchem-1251	332	30	the	the	DET
eurjchem-1251	332	31	experimental	experimental	ADJ
eurjchem-1251	332	32	part	part	NOUN
eurjchem-1251	332	33	.	.	PUNCT
eurjchem-1251	333	1	reaction	reaction	NOUN
eurjchem-1251	333	2	of	of	ADP
eurjchem-1251	333	3	the	the	DET
eurjchem-1251	333	4	3‐aminopyridazine(5	3‐aminopyridazine(5	NUM
eurjchem-1251	333	5	)	)	PUNCT
eurjchem-1251	333	6	with	with	ADP
eurjchem-1251	333	7	aromatic	aromatic	ADJ
eurjchem-1251	333	8	aldehydes	aldehyde	NOUN
eurjchem-1251	333	9	under	under	ADP
eurjchem-1251	333	10	different	different	ADJ
eurjchem-1251	333	11	reaction	reaction	NOUN
eurjchem-1251	333	12	conditions	condition	NOUN
eurjchem-1251	333	13	did	do	AUX
eurjchem-1251	333	14	not	not	PART
eurjchem-1251	333	15	produce	produce	VERB
eurjchem-1251	333	16	the	the	DET
eurjchem-1251	333	17	arylidene	arylidene	NOUN
eurjchem-1251	333	18	amino	amino	NOUN
eurjchem-1251	333	19	derivatives	derivative	NOUN
eurjchem-1251	333	20	,	,	PUNCT
eurjchem-1251	333	21	but	but	CCONJ
eurjchem-1251	333	22	led	lead	VERB
eurjchem-1251	333	23	only	only	ADV
eurjchem-1251	333	24	to	to	ADP
eurjchem-1251	333	25	the	the	DET
eurjchem-1251	333	26	recovery	recovery	NOUN
eurjchem-1251	333	27	of	of	ADP
eurjchem-1251	333	28	the	the	DET
eurjchem-1251	333	29	starting	starting	NOUN
eurjchem-1251	333	30	material	material	NOUN
eurjchem-1251	333	31	,	,	PUNCT
eurjchem-1251	333	32	possibly	possibly	ADV
eurjchem-1251	333	33	owing	owe	VERB
eurjchem-1251	333	34	to	to	ADP
eurjchem-1251	333	35	steric	steric	ADJ
eurjchem-1251	333	36	hindrance	hindrance	NOUN
eurjchem-1251	333	37	of	of	ADP
eurjchem-1251	333	38	the	the	DET
eurjchem-1251	333	39	bulky	bulky	ADJ
eurjchem-1251	333	40	phenyl	phenyl	NOUN
eurjchem-1251	333	41	group	group	NOUN
eurjchem-1251	333	42	in	in	ADP
eurjchem-1251	333	43	position	position	NOUN
eurjchem-1251	333	44	four	four	NUM
eurjchem-1251	333	45	,	,	PUNCT
eurjchem-1251	333	46	and	and	CCONJ
eurjchem-1251	333	47	the	the	DET
eurjchem-1251	333	48	electronic	electronic	ADJ
eurjchem-1251	333	49	effect	effect	NOUN
eurjchem-1251	333	50	of	of	ADP
eurjchem-1251	333	51	sp2	sp2	NOUN
eurjchem-1251	333	52	cyclic	cyclic	ADJ
eurjchem-1251	333	53	nitrogen	nitrogen	NOUN
eurjchem-1251	333	54	atom	atom	NOUN
eurjchem-1251	333	55	.	.	PUNCT
eurjchem-1251	334	1	on	on	ADP
eurjchem-1251	334	2	the	the	DET
eurjchem-1251	334	3	other	other	ADJ
eurjchem-1251	334	4	hand	hand	NOUN
eurjchem-1251	334	5	,	,	PUNCT
eurjchem-1251	334	6	refluxing	refluxing	NOUN
eurjchem-1251	334	7	compound	compound	NOUN
eurjchem-1251	334	8	5	5	NUM
eurjchem-1251	334	9	with	with	ADP
eurjchem-1251	334	10	little	little	ADJ
eurjchem-1251	334	11	excess	excess	NOUN
eurjchem-1251	334	12	of	of	ADP
eurjchem-1251	334	13	acetaldehyde	acetaldehyde	NOUN
eurjchem-1251	334	14	for	for	ADP
eurjchem-1251	334	15	4	4	NUM
eurjchem-1251	334	16	hours	hour	NOUN
eurjchem-1251	334	17	afforded	afford	VERB
eurjchem-1251	334	18	n‐	n‐	NOUN
eurjchem-1251	334	19	ethylidene‐4,5,6‐triphenylpyridazin‐3‐amine	ethylidene‐4,5,6‐triphenylpyridazin‐3‐amine	PROPN
eurjchem-1251	334	20	(	(	PUNCT
eurjchem-1251	334	21	7	7	NUM
eurjchem-1251	334	22	)	)	PUNCT
eurjchem-1251	334	23	(	(	PUNCT
eurjchem-1251	334	24	scheme	scheme	NOUN
eurjchem-1251	334	25	2	2	NUM
eurjchem-1251	334	26	)	)	PUNCT
eurjchem-1251	334	27	,	,	PUNCT
eurjchem-1251	334	28	as	as	SCONJ
eurjchem-1251	334	29	proved	prove	VERB
eurjchem-1251	334	30	by	by	ADP
eurjchem-1251	334	31	the	the	DET
eurjchem-1251	334	32	disappearance	disappearance	NOUN
eurjchem-1251	334	33	of	of	ADP
eurjchem-1251	334	34	nh2	nh2	NOUN
eurjchem-1251	334	35	bands	band	NOUN
eurjchem-1251	334	36	of	of	ADP
eurjchem-1251	334	37	the	the	DET
eurjchem-1251	334	38	starting	starting	NOUN
eurjchem-1251	334	39	material	material	NOUN
eurjchem-1251	334	40	in	in	ADP
eurjchem-1251	334	41	ir	ir	PROPN
eurjchem-1251	334	42	and	and	CCONJ
eurjchem-1251	334	43	1h	1h	NUM
eurjchem-1251	334	44	nmr	nmr	PROPN
eurjchem-1251	334	45	spectra	spectra	PROPN
eurjchem-1251	334	46	.	.	PUNCT
eurjchem-1251	335	1	the	the	DET
eurjchem-1251	335	2	reaction	reaction	NOUN
eurjchem-1251	335	3	of	of	ADP
eurjchem-1251	335	4	compound	compound	NOUN
eurjchem-1251	335	5	5	5	NUM
eurjchem-1251	335	6	with	with	ADP
eurjchem-1251	335	7	active	active	ADJ
eurjchem-1251	335	8	methylene	methylene	NOUN
eurjchem-1251	335	9	compoundswas	compoundswas	AUX
eurjchem-1251	335	10	investigated	investigate	VERB
eurjchem-1251	335	11	,	,	PUNCT
eurjchem-1251	335	12	such	such	ADJ
eurjchem-1251	335	13	as	as	ADP
eurjchem-1251	335	14	diethyl	diethyl	NOUN
eurjchem-1251	335	15	malonate	malonate	NOUN
eurjchem-1251	335	16	at	at	ADP
eurjchem-1251	335	17	refluxing	refluxing	NOUN
eurjchem-1251	335	18	temperature	temperature	NOUN
eurjchem-1251	335	19	for	for	ADP
eurjchem-1251	335	20	3	3	NUM
eurjchem-1251	335	21	hours	hour	NOUN
eurjchem-1251	335	22	gave	give	VERB
eurjchem-1251	335	23	the	the	DET
eurjchem-1251	335	24	dimeric	dimeric	ADJ
eurjchem-1251	335	25	structure	structure	NOUN
eurjchem-1251	335	26	8	8	NUM
eurjchem-1251	335	27	(	(	PUNCT
eurjchem-1251	335	28	scheme	scheme	NOUN
eurjchem-1251	335	29	2	2	NUM
eurjchem-1251	335	30	)	)	PUNCT
eurjchem-1251	335	31	as	as	SCONJ
eurjchem-1251	335	32	indicated	indicate	VERB
eurjchem-1251	335	33	from	from	ADP
eurjchem-1251	335	34	elemental	elemental	ADJ
eurjchem-1251	335	35	analysis	analysis	NOUN
eurjchem-1251	335	36	and	and	CCONJ
eurjchem-1251	335	37	spectral	spectral	ADJ
eurjchem-1251	335	38	data	datum	NOUN
eurjchem-1251	335	39	(	(	PUNCT
eurjchem-1251	335	40	ir	ir	PROPN
eurjchem-1251	335	41	,	,	PUNCT
eurjchem-1251	335	42	mass	mass	PROPN
eurjchem-1251	335	43	,	,	PUNCT
eurjchem-1251	335	44	and	and	CCONJ
eurjchem-1251	335	45	1h	1h	NUM
eurjchem-1251	335	46	nmr	nmr	PROPN
eurjchem-1251	335	47	spectra	spectra	PROPN
eurjchem-1251	335	48	)	)	PUNCT
eurjchem-1251	335	49	.	.	PUNCT
eurjchem-1251	336	1	on	on	ADP
eurjchem-1251	336	2	the	the	DET
eurjchem-1251	336	3	other	other	ADJ
eurjchem-1251	336	4	hand	hand	NOUN
eurjchem-1251	336	5	,	,	PUNCT
eurjchem-1251	336	6	reaction	reaction	NOUN
eurjchem-1251	336	7	of	of	ADP
eurjchem-1251	336	8	compound	compound	NOUN
eurjchem-1251	336	9	5	5	NUM
eurjchem-1251	336	10	with	with	ADP
eurjchem-1251	336	11	malonic	malonic	ADJ
eurjchem-1251	336	12	acid	acid	NOUN
eurjchem-1251	336	13	in	in	ADP
eurjchem-1251	336	14	presence	presence	NOUN
eurjchem-1251	336	15	of	of	ADP
eurjchem-1251	336	16	phosphoryl	phosphoryl	PROPN
eurjchem-1251	336	17	chloride	chloride	PROPN
eurjchem-1251	336	18	at	at	ADP
eurjchem-1251	336	19	refluxing	refluxing	NOUN
eurjchem-1251	336	20	tempe‐	tempe‐	PUNCT
eurjchem-1251	336	21	rature	rature	NOUN
eurjchem-1251	336	22	for	for	ADP
eurjchem-1251	336	23	1	1	NUM
eurjchem-1251	336	24	hour	hour	NOUN
eurjchem-1251	336	25	afforded	afford	VERB
eurjchem-1251	336	26	7,8,9‐triphenyl‐2h‐pyrimido[1,2‐	7,8,9‐triphenyl‐2h‐pyrimido[1,2‐	NOUN
eurjchem-1251	336	27	b]pyridazine‐2,4(3h)‐dione	b]pyridazine‐2,4(3h)‐dione	NOUN
eurjchem-1251	336	28	(	(	PUNCT
eurjchem-1251	336	29	9	9	NUM
eurjchem-1251	336	30	)	)	PUNCT
eurjchem-1251	336	31	in	in	ADP
eurjchem-1251	336	32	good	good	ADJ
eurjchem-1251	336	33	yield	yield	NOUN
eurjchem-1251	336	34	.	.	PUNCT
eurjchem-1251	337	1	deeb	deeb	PROPN
eurjchem-1251	337	2	et	et	PROPN
eurjchem-1251	337	3	al	al	PROPN
eurjchem-1251	337	4	.	.	PUNCT
eurjchem-1251	337	5	/	/	SYM
eurjchem-1251	337	6	european	european	PROPN
eurjchem-1251	337	7	journal	journal	PROPN
eurjchem-1251	337	8	of	of	ADP
eurjchem-1251	337	9	chemistry	chemistry	NOUN
eurjchem-1251	337	10	6	6	NUM
eurjchem-1251	337	11	(	(	PUNCT
eurjchem-1251	337	12	2	2	NUM
eurjchem-1251	337	13	)	)	PUNCT
eurjchem-1251	337	14	(	(	PUNCT
eurjchem-1251	337	15	2015	2015	NUM
eurjchem-1251	337	16	)	)	PUNCT
eurjchem-1251	337	17	211‐218	211‐218	NOUN
eurjchem-1251	337	18	217	217	NUM
eurjchem-1251	337	19	table	table	NOUN
eurjchem-1251	337	20	1	1	NUM
eurjchem-1251	337	21	.	.	PUNCT
eurjchem-1251	337	22	antimicrobial	antimicrobial	ADJ
eurjchem-1251	337	23	activity	activity	NOUN
eurjchem-1251	337	24	of	of	ADP
eurjchem-1251	337	25	the	the	DET
eurjchem-1251	337	26	prepared	prepare	VERB
eurjchem-1251	337	27	compounds	compound	NOUN
eurjchem-1251	337	28	*	*	NOUN
eurjchem-1251	337	29	.	.	PUNCT
eurjchem-1251	338	1	zone	zone	NOUN
eurjchem-1251	338	2	of	of	ADP
eurjchem-1251	338	3	inhibition	inhibition	NOUN
eurjchem-1251	338	4	compound	compound	NOUN
eurjchem-1251	338	5	aspergillus	aspergillus	NOUN
eurjchem-1251	338	6	niger	niger	NOUN
eurjchem-1251	338	7	candida	candida	NOUN
eurjchem-1251	338	8	albicans	albican	NOUN
eurjchem-1251	338	9	pseudomonas	pseudomona	NOUN
eurjchem-1251	338	10	aeruginosa	aeruginosa	NOUN
eurjchem-1251	338	11	(	(	PUNCT
eurjchem-1251	338	12	g‐	g‐	NOUN
eurjchem-1251	338	13	)	)	PUNCT
eurjchem-1251	338	14	escherichia	escherichia	NOUN
eurjchem-1251	338	15	coli	coli	NOUN
eurjchem-1251	338	16	(	(	PUNCT
eurjchem-1251	338	17	g‐	g‐	NOUN
eurjchem-1251	338	18	)	)	PUNCT
eurjchem-1251	338	19	bacillus	bacillus	NOUN
eurjchem-1251	338	20	subtilis	subtili	NOUN
eurjchem-1251	338	21	(	(	PUNCT
eurjchem-1251	338	22	g+	g+	NOUN
eurjchem-1251	338	23	)	)	PUNCT
eurjchem-1251	338	24	staphylococcus	staphylococcus	NOUN
eurjchem-1251	338	25	aureus	aureus	NOUN
eurjchem-1251	338	26	(	(	PUNCT
eurjchem-1251	338	27	g+	g+	NOUN
eurjchem-1251	338	28	)	)	PUNCT
eurjchem-1251	338	29	‐	‐	NOUN
eurjchem-1251	338	30	‐+++++	‐+++++	PUNCT
eurjchem-1251	339	1	+	+	PROPN
eurjchem-1251	339	2	+	+	ADJ
eurjchem-1251	339	3	+	+	ADJ
eurjchem-1251	339	4	+	+	ADJ
eurjchem-1251	339	5	+	+	ADJ
eurjchem-1251	339	6	5	5	NUM
eurjchem-1251	339	7	+	+	ADJ
eurjchem-1251	339	8	+	+	ADJ
eurjchem-1251	339	9	+	+	ADJ
eurjchem-1251	339	10	+	+	ADJ
eurjchem-1251	339	11	+	+	ADJ
eurjchem-1251	339	12	+	+	ADJ
eurjchem-1251	339	13	+	+	ADJ
eurjchem-1251	339	14	+	+	ADJ
eurjchem-1251	339	15	+	+	ADJ
eurjchem-1251	339	16	‐	‐	ADJ
eurjchem-1251	339	17	+	+	NOUN
eurjchem-1251	339	18	6b	6b	NOUN
eurjchem-1251	340	1	+	+	PROPN
eurjchem-1251	340	2	+	+	ADJ
eurjchem-1251	340	3	+	+	ADJ
eurjchem-1251	340	4	+	+	ADJ
eurjchem-1251	340	5	+	+	ADJ
eurjchem-1251	340	6	+	+	ADJ
eurjchem-1251	340	7	+	+	ADJ
eurjchem-1251	340	8	+	+	ADJ
eurjchem-1251	340	9	+	+	ADJ
eurjchem-1251	340	10	+	+	ADJ
eurjchem-1251	340	11	+	+	ADJ
eurjchem-1251	340	12	+	+	ADJ
eurjchem-1251	340	13	+	+	ADJ
eurjchem-1251	340	14	+	+	ADJ
eurjchem-1251	340	15	+	+	ADJ
eurjchem-1251	340	16	9	9	NUM
eurjchem-1251	340	17	+	+	ADJ
eurjchem-1251	340	18	+	+	ADJ
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eurjchem-1251	340	20	+	+	ADJ
eurjchem-1251	340	21	+	+	ADJ
eurjchem-1251	340	22	+	+	ADJ
eurjchem-1251	340	23	+	+	ADJ
eurjchem-1251	340	24	+	+	ADJ
eurjchem-1251	340	25	+	+	ADJ
eurjchem-1251	340	26	+	+	ADJ
eurjchem-1251	340	27	+	+	ADJ
eurjchem-1251	340	28	+	+	ADJ
eurjchem-1251	340	29	+	+	ADJ
eurjchem-1251	340	30	+	+	ADJ
eurjchem-1251	340	31	+	+	ADJ
eurjchem-1251	340	32	+	+	NOUN
eurjchem-1251	340	33	11a	11a	NOUN
eurjchem-1251	340	34	+	+	PUNCT
eurjchem-1251	340	35	+	+	PROPN
eurjchem-1251	340	36	+	+	ADJ
eurjchem-1251	340	37	+	+	NOUN
eurjchem-1251	340	38	+	+	NOUN
eurjchem-1251	340	39	‐‐+	‐‐+	NOUN
eurjchem-1251	341	1	+	+	PROPN
eurjchem-1251	341	2	+	+	PROPN
eurjchem-1251	341	3	15a	15a	NOUN
eurjchem-1251	341	4	+	+	PUNCT
eurjchem-1251	341	5	+	+	PROPN
eurjchem-1251	341	6	+	+	ADJ
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eurjchem-1251	341	8	+	+	ADJ
eurjchem-1251	341	9	+	+	ADJ
eurjchem-1251	341	10	+	+	ADJ
eurjchem-1251	341	11	+	+	ADJ
eurjchem-1251	341	12	+	+	ADJ
eurjchem-1251	341	13	+	+	ADJ
eurjchem-1251	341	14	+	+	ADJ
eurjchem-1251	342	1	+	+	ADJ
eurjchem-1251	342	2	+	+	NOUN
eurjchem-1251	342	3	15b	15b	NOUN
eurjchem-1251	342	4	+	+	ADJ
eurjchem-1251	342	5	+	+	ADJ
eurjchem-1251	342	6	+	+	ADJ
eurjchem-1251	342	7	+	+	ADJ
eurjchem-1251	342	8	+	+	ADJ
eurjchem-1251	342	9	+	+	ADJ
eurjchem-1251	342	10	+	+	ADJ
eurjchem-1251	342	11	+	+	ADJ
eurjchem-1251	342	12	+	+	ADJ
eurjchem-1251	342	13	+	+	ADJ
eurjchem-1251	342	14	+	+	ADJ
eurjchem-1251	342	15	+	+	ADJ
eurjchem-1251	342	16	+	+	ADJ
eurjchem-1251	342	17	+	+	ADJ
eurjchem-1251	342	18	+	+	NOUN
eurjchem-1251	342	19	15c	15c	NOUN
eurjchem-1251	342	20	+	+	PUNCT
eurjchem-1251	342	21	+	+	ADJ
eurjchem-1251	342	22	+	+	ADJ
eurjchem-1251	342	23	+	+	ADJ
eurjchem-1251	342	24	+	+	ADJ
eurjchem-1251	342	25	+	+	ADJ
eurjchem-1251	342	26	+	+	ADJ
eurjchem-1251	342	27	+	+	ADJ
eurjchem-1251	342	28	+	+	ADJ
eurjchem-1251	342	29	+	+	ADJ
eurjchem-1251	342	30	+	+	ADJ
eurjchem-1251	342	31	+	+	ADJ
eurjchem-1251	342	32	+	+	ADJ
eurjchem-1251	342	33	+	+	ADJ
eurjchem-1251	342	34	+	+	ADJ
eurjchem-1251	342	35	+	+	ADJ
eurjchem-1251	342	36	+	+	NOUN
eurjchem-1251	342	37	15d	15d	NOUN
eurjchem-1251	342	38	‐	‐	ADP
eurjchem-1251	342	39	‐+++++++++	‐+++++++++	PUNCT
eurjchem-1251	342	40	+	+	PROPN
eurjchem-1251	342	41	+	+	ADJ
eurjchem-1251	342	42	+	+	NOUN
eurjchem-1251	342	43	15e	15e	NOUN
eurjchem-1251	342	44	+	+	PROPN
eurjchem-1251	342	45	+	+	PROPN
eurjchem-1251	342	46	+	+	ADJ
eurjchem-1251	342	47	+	+	ADJ
eurjchem-1251	342	48	+	+	ADJ
eurjchem-1251	342	49	+	+	ADJ
eurjchem-1251	342	50	+	+	ADJ
eurjchem-1251	342	51	+	+	ADJ
eurjchem-1251	342	52	+	+	ADJ
eurjchem-1251	342	53	+	+	ADJ
eurjchem-1251	342	54	+	+	ADJ
eurjchem-1251	342	55	+	+	ADJ
eurjchem-1251	342	56	+	+	ADJ
eurjchem-1251	342	57	+	+	ADJ
eurjchem-1251	342	58	+	+	ADJ
eurjchem-1251	342	59	+	+	ADJ
eurjchem-1251	342	60	15f	15f	NOUN
eurjchem-1251	342	61	‐	‐	ADV
eurjchem-1251	342	62	‐++++++	‐++++++	PUNCT
eurjchem-1251	342	63	+	+	PROPN
eurjchem-1251	342	64	+	+	ADJ
eurjchem-1251	342	65	+	+	ADJ
eurjchem-1251	342	66	+	+	ADJ
eurjchem-1251	342	67	+	+	ADJ
eurjchem-1251	342	68	15	15	NUM
eurjchem-1251	342	69	g	g	NOUN
eurjchem-1251	342	70	‐	‐	NOUN
eurjchem-1251	342	71	‐	‐	ADV
eurjchem-1251	342	72	+	+	PROPN
eurjchem-1251	342	73	+	+	ADJ
eurjchem-1251	342	74	+	+	ADJ
eurjchem-1251	342	75	+	+	ADJ
eurjchem-1251	342	76	+	+	ADJ
eurjchem-1251	342	77	+	+	ADJ
eurjchem-1251	342	78	+	+	ADJ
eurjchem-1251	342	79	+	+	ADJ
eurjchem-1251	342	80	+	+	ADJ
eurjchem-1251	342	81	+	+	ADJ
eurjchem-1251	342	82	+	+	ADJ
eurjchem-1251	342	83	+	+	ADJ
eurjchem-1251	342	84	+	+	ADJ
eurjchem-1251	342	85	+	+	ADJ
eurjchem-1251	342	86	+	+	ADJ
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eurjchem-1251	342	88	d.s	d.s	PROPN
eurjchem-1251	342	89	.	.	PROPN
eurjchem-1251	343	1	+	+	PROPN
eurjchem-1251	343	2	+	+	ADJ
eurjchem-1251	343	3	+	+	ADJ
eurjchem-1251	343	4	+	+	ADJ
eurjchem-1251	343	5	+	+	ADJ
eurjchem-1251	343	6	+	+	ADJ
eurjchem-1251	343	7	+	+	ADJ
eurjchem-1251	343	8	+	+	ADJ
eurjchem-1251	343	9	‐	‐	NOUN
eurjchem-1251	343	10	‐	‐	ADV
eurjchem-1251	343	11	‐	‐	ADV
eurjchem-1251	343	12	‐	‐	ADJ
eurjchem-1251	343	13	fungistatin	fungistatin	NOUN
eurjchem-1251	343	14	*	*	PUNCT
eurjchem-1251	343	15	the	the	DET
eurjchem-1251	343	16	concentration	concentration	NOUN
eurjchem-1251	343	17	ofthe	ofthe	NOUN
eurjchem-1251	343	18	all	all	DET
eurjchem-1251	343	19	synthesised	synthesise	VERB
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eurjchem-1251	343	23	two	two	NUM
eurjchem-1251	343	24	references	reference	NOUN
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eurjchem-1251	343	30	ml	ml	NOUN
eurjchem-1251	343	31	of	of	ADP
eurjchem-1251	343	32	dimethylformamide	dimethylformamide	NOUN
eurjchem-1251	343	33	.	.	PUNCT
eurjchem-1251	344	1	zone	zone	NOUN
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eurjchem-1251	344	4	:	:	PUNCT
eurjchem-1251	344	5	+	+	CCONJ
eurjchem-1251	344	6	=	=	SYM
eurjchem-1251	344	7	<	<	X
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eurjchem-1251	344	10	;	;	PUNCT
eurjchem-1251	344	11	+	+	PROPN
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eurjchem-1251	344	13	=	=	SYM
eurjchem-1251	344	14	15‐24	15‐24	NUM
eurjchem-1251	344	15	mm	mm	NOUN
eurjchem-1251	344	16	;	;	PUNCT
eurjchem-1251	345	1	+	+	PROPN
eurjchem-1251	345	2	+	+	ADJ
eurjchem-1251	345	3	+	+	X
eurjchem-1251	345	4	=	=	SYM
eurjchem-1251	345	5	25‐34	25‐34	NUM
eurjchem-1251	345	6	mm	mm	NOUN
eurjchem-1251	345	7	;	;	PUNCT
eurjchem-1251	346	1	+	+	PROPN
eurjchem-1251	346	2	+	+	ADJ
eurjchem-1251	346	3	+	+	ADJ
eurjchem-1251	346	4	+	+	VERB
eurjchem-1251	346	5	=	=	NOUN
eurjchem-1251	346	6	35‐44	35‐44	NUM
eurjchem-1251	346	7	mm	mm	NOUN
eurjchem-1251	346	8	;	;	PUNCT
eurjchem-1251	346	9	+	+	PROPN
eurjchem-1251	346	10	+	+	ADJ
eurjchem-1251	346	11	+	+	ADJ
eurjchem-1251	346	12	+	+	ADJ
eurjchem-1251	346	13	+	+	ADJ
eurjchem-1251	346	14	=	=	SYM
eurjchem-1251	346	15	45‐54	45‐54	NUM
eurjchem-1251	346	16	mm	mm	NOUN
eurjchem-1251	346	17	,	,	PUNCT
eurjchem-1251	346	18	‐	‐	NOUN
eurjchem-1251	346	19	=	=	NOUN
eurjchem-1251	346	20	no	no	DET
eurjchem-1251	346	21	inhibition	inhibition	NOUN
eurjchem-1251	346	22	.	.	PUNCT
eurjchem-1251	347	1	however	however	ADV
eurjchem-1251	347	2	,	,	PUNCT
eurjchem-1251	347	3	when	when	SCONJ
eurjchem-1251	347	4	compound	compound	NOUN
eurjchem-1251	347	5	5was	5was	PROPN
eurjchem-1251	347	6	refluxed	refluxe	VERB
eurjchem-1251	347	7	in	in	ADP
eurjchem-1251	347	8	diethyl	diethyl	NOUN
eurjchem-1251	347	9	oxalate	oxalate	NOUN
eurjchem-1251	347	10	,	,	PUNCT
eurjchem-1251	347	11	a	a	DET
eurjchem-1251	347	12	product	product	NOUN
eurjchem-1251	347	13	was	be	AUX
eurjchem-1251	347	14	isolated	isolate	VERB
eurjchem-1251	347	15	in	in	ADP
eurjchem-1251	347	16	80	80	NUM
eurjchem-1251	347	17	%	%	NOUN
eurjchem-1251	347	18	yield	yield	NOUN
eurjchem-1251	347	19	,	,	PUNCT
eurjchem-1251	347	20	which	which	PRON
eurjchem-1251	347	21	was	be	AUX
eurjchem-1251	347	22	proved	prove	VERB
eurjchem-1251	347	23	to	to	PART
eurjchem-1251	347	24	be	be	AUX
eurjchem-1251	347	25	ethyl	ethyl	PROPN
eurjchem-1251	347	26	oxo[(4,5,6‐triphenylpyridazin‐3‐yl	oxo[(4,5,6‐triphenylpyridazin‐3‐yl	NUM
eurjchem-1251	347	27	)	)	PUNCT
eurjchem-1251	347	28	amino]acetate	amino]acetate	PROPN
eurjchem-1251	347	29	,	,	PUNCT
eurjchem-1251	347	30	10a	10a	X
eurjchem-1251	347	31	(	(	PUNCT
eurjchem-1251	347	32	scheme	scheme	NOUN
eurjchem-1251	347	33	3	3	NUM
eurjchem-1251	347	34	)	)	PUNCT
eurjchem-1251	347	35	on	on	ADP
eurjchem-1251	347	36	the	the	DET
eurjchem-1251	347	37	basis	basis	NOUN
eurjchem-1251	347	38	of	of	ADP
eurjchem-1251	347	39	elemental	elemental	ADJ
eurjchem-1251	347	40	and	and	CCONJ
eurjchem-1251	347	41	spectral	spectral	ADJ
eurjchem-1251	347	42	data	datum	NOUN
eurjchem-1251	347	43	.	.	PUNCT
eurjchem-1251	348	1	refluxing	refluxing	NOUN
eurjchem-1251	348	2	compound	compound	NOUN
eurjchem-1251	348	3	5	5	NUM
eurjchem-1251	348	4	with	with	ADP
eurjchem-1251	348	5	ethyl	ethyl	PROPN
eurjchem-1251	348	6	cyanoacetate	cyanoacetate	NOUN
eurjchem-1251	348	7	produced	produce	VERB
eurjchem-1251	348	8	2‐cyano‐n‐(4,5,6‐triphenyl	2‐cyano‐n‐(4,5,6‐triphenyl	NUM
eurjchem-1251	348	9	pyridazin‐3‐yl	pyridazin‐3‐yl	NUM
eurjchem-1251	348	10	)	)	PUNCT
eurjchem-1251	348	11	acet‐	acet‐	PROPN
eurjchem-1251	349	1	amide	amide	NOUN
eurjchem-1251	349	2	10b	10b	NOUN
eurjchem-1251	349	3	(	(	PUNCT
eurjchem-1251	349	4	scheme	scheme	NOUN
eurjchem-1251	349	5	3	3	NUM
eurjchem-1251	349	6	)	)	PUNCT
eurjchem-1251	349	7	,	,	PUNCT
eurjchem-1251	349	8	as	as	SCONJ
eurjchem-1251	349	9	proved	prove	VERB
eurjchem-1251	349	10	by	by	ADP
eurjchem-1251	349	11	the	the	DET
eurjchem-1251	349	12	presence	presence	NOUN
eurjchem-1251	349	13	of	of	ADP
eurjchem-1251	349	14	cyano	cyano	NOUN
eurjchem-1251	349	15	group	group	NOUN
eurjchem-1251	349	16	at	at	ADP
eurjchem-1251	349	17	2204	2204	NUM
eurjchem-1251	349	18	cm‐1	cm‐1	NOUN
eurjchem-1251	349	19	and	and	CCONJ
eurjchem-1251	349	20	amide	amide	NOUN
eurjchem-1251	349	21	carbonyl	carbonyl	NOUN
eurjchem-1251	349	22	group	group	NOUN
eurjchem-1251	349	23	at	at	ADP
eurjchem-1251	349	24	1658	1658	NUM
eurjchem-1251	349	25	cm‐1	cm‐1	NOUN
eurjchem-1251	349	26	,	,	PUNCT
eurjchem-1251	349	27	and	and	CCONJ
eurjchem-1251	349	28	the	the	DET
eurjchem-1251	349	29	disappearance	disappearance	NOUN
eurjchem-1251	349	30	of	of	ADP
eurjchem-1251	349	31	the	the	DET
eurjchem-1251	349	32	nh2	nh2	NOUN
eurjchem-1251	349	33	bands	band	NOUN
eurjchem-1251	349	34	in	in	ADP
eurjchem-1251	349	35	the	the	DET
eurjchem-1251	349	36	ir	ir	PROPN
eurjchem-1251	349	37	spectrum	spectrum	NOUN
eurjchem-1251	349	38	.	.	PUNCT
eurjchem-1251	350	1	on	on	ADP
eurjchem-1251	350	2	the	the	DET
eurjchem-1251	350	3	other	other	ADJ
eurjchem-1251	350	4	hand	hand	NOUN
eurjchem-1251	350	5	,	,	PUNCT
eurjchem-1251	350	6	heating	heat	VERB
eurjchem-1251	350	7	equimolar	equimolar	NOUN
eurjchem-1251	350	8	amounts	amount	NOUN
eurjchem-1251	350	9	of	of	ADP
eurjchem-1251	350	10	compound	compound	NOUN
eurjchem-1251	350	11	5	5	NUM
eurjchem-1251	350	12	and	and	CCONJ
eurjchem-1251	350	13	ethyl	ethyl	PROPN
eurjchem-1251	350	14	cyanoacetate	cyanoacetate	NOUN
eurjchem-1251	350	15	in	in	ADP
eurjchem-1251	350	16	polyphosphoric	polyphosphoric	ADJ
eurjchem-1251	350	17	acid	acid	NOUN
eurjchem-1251	350	18	at	at	ADP
eurjchem-1251	350	19	110	110	NUM
eurjchem-1251	350	20	°	°	NOUN
eurjchem-1251	350	21	c	c	NOUN
eurjchem-1251	350	22	for	for	ADP
eurjchem-1251	350	23	6	6	NUM
eurjchem-1251	350	24	hours	hour	NOUN
eurjchem-1251	350	25	,	,	PUNCT
eurjchem-1251	350	26	quenching	quench	VERB
eurjchem-1251	350	27	the	the	DET
eurjchem-1251	350	28	reaction	reaction	NOUN
eurjchem-1251	350	29	mixture	mixture	NOUN
eurjchem-1251	350	30	with	with	ADP
eurjchem-1251	350	31	water	water	NOUN
eurjchem-1251	350	32	,	,	PUNCT
eurjchem-1251	350	33	and	and	CCONJ
eurjchem-1251	350	34	neutralizing	neutralize	VERB
eurjchem-1251	350	35	with	with	ADP
eurjchem-1251	350	36	10	10	NUM
eurjchem-1251	350	37	%	%	NOUN
eurjchem-1251	350	38	sodium	sodium	NOUN
eurjchem-1251	350	39	hydroxide	hydroxide	NOUN
eurjchem-1251	350	40	,	,	PUNCT
eurjchem-1251	350	41	yielding	yield	VERB
eurjchem-1251	350	42	4‐amino‐7	4‐amino‐7	PROPN
eurjchem-1251	350	43	,	,	PUNCT
eurjchem-1251	350	44	8	8	NUM
eurjchem-1251	350	45	,	,	PUNCT
eurjchem-1251	350	46	9‐triphenyl‐2h‐pyrimido[1,2‐b]pyridazin‐2‐one	9‐triphenyl‐2h‐pyrimido[1,2‐b]pyridazin‐2‐one	NUM
eurjchem-1251	350	47	(	(	PUNCT
eurjchem-1251	350	48	11a	11a	NOUN
eurjchem-1251	350	49	)	)	PUNCT
eurjchem-1251	350	50	,	,	PUNCT
eurjchem-1251	350	51	which	which	PRON
eurjchem-1251	350	52	was	be	AUX
eurjchem-1251	350	53	identified	identify	VERB
eurjchem-1251	350	54	on	on	ADP
eurjchem-1251	350	55	the	the	DET
eurjchem-1251	350	56	basis	basis	NOUN
eurjchem-1251	350	57	of	of	ADP
eurjchem-1251	350	58	elemental	elemental	ADJ
eurjchem-1251	350	59	analysis	analysis	NOUN
eurjchem-1251	350	60	and	and	CCONJ
eurjchem-1251	350	61	spectral	spectral	ADJ
eurjchem-1251	350	62	data	datum	NOUN
eurjchem-1251	350	63	.	.	PUNCT
eurjchem-1251	351	1	the	the	DET
eurjchem-1251	351	2	reaction	reaction	NOUN
eurjchem-1251	351	3	of	of	ADP
eurjchem-1251	351	4	the	the	DET
eurjchem-1251	351	5	4‐aminopyrimidopyridazine11a	4‐aminopyrimidopyridazine11a	NOUN
eurjchem-1251	351	6	with	with	ADP
eurjchem-1251	351	7	acetic	acetic	ADJ
eurjchem-1251	351	8	anhydride	anhydride	NOUN
eurjchem-1251	351	9	produced	produce	VERB
eurjchem-1251	351	10	the	the	DET
eurjchem-1251	351	11	corresponding	correspond	VERB
eurjchem-1251	351	12	4‐acetylamino	4‐acetylamino	PROPN
eurjchem-1251	351	13	derivative	derivative	ADJ
eurjchem-1251	351	14	11b	11b	NOUN
eurjchem-1251	351	15	(	(	PUNCT
eurjchem-1251	351	16	scheme	scheme	NOUN
eurjchem-1251	351	17	3	3	NUM
eurjchem-1251	351	18	)	)	PUNCT
eurjchem-1251	351	19	,	,	PUNCT
eurjchem-1251	351	20	which	which	PRON
eurjchem-1251	351	21	affords	afford	VERB
eurjchem-1251	351	22	a	a	DET
eurjchem-1251	351	23	further	further	ADJ
eurjchem-1251	351	24	evidence	evidence	NOUN
eurjchem-1251	351	25	for	for	ADP
eurjchem-1251	351	26	the	the	DET
eurjchem-1251	351	27	structure	structure	NOUN
eurjchem-1251	351	28	of	of	ADP
eurjchem-1251	351	29	the	the	DET
eurjchem-1251	351	30	compound	compound	NOUN
eurjchem-1251	351	31	11a	11a	NOUN
eurjchem-1251	351	32	.	.	PUNCT
eurjchem-1251	352	1	fusion	fusion	NOUN
eurjchem-1251	352	2	of	of	ADP
eurjchem-1251	352	3	the	the	DET
eurjchem-1251	352	4	3‐aminopyridazine	3‐aminopyridazine	NUM
eurjchem-1251	352	5	derivative	derivative	NOUN
eurjchem-1251	352	6	5	5	NUM
eurjchem-1251	352	7	with	with	ADP
eurjchem-1251	352	8	ethyl	ethyl	PROPN
eurjchem-1251	352	9	acetoacetate	acetoacetate	NOUN
eurjchem-1251	352	10	was	be	AUX
eurjchem-1251	352	11	found	find	VERB
eurjchem-1251	352	12	to	to	PART
eurjchem-1251	352	13	proceed	proceed	VERB
eurjchem-1251	352	14	steadily	steadily	ADV
eurjchem-1251	352	15	to	to	PART
eurjchem-1251	352	16	give	give	VERB
eurjchem-1251	352	17	the	the	DET
eurjchem-1251	352	18	condensation	condensation	NOUN
eurjchem-1251	352	19	product	product	NOUN
eurjchem-1251	352	20	12a	12a	NOUN
eurjchem-1251	352	21	(	(	PUNCT
eurjchem-1251	352	22	scheme	scheme	NOUN
eurjchem-1251	352	23	3	3	NUM
eurjchem-1251	352	24	)	)	PUNCT
eurjchem-1251	352	25	.	.	PUNCT
eurjchem-1251	353	1	the	the	DET
eurjchem-1251	353	2	ir	ir	PROPN
eurjchem-1251	353	3	spectrum	spectrum	NOUN
eurjchem-1251	353	4	of	of	ADP
eurjchem-1251	353	5	compound	compound	NOUN
eurjchem-1251	353	6	12a	12a	NOUN
eurjchem-1251	353	7	showed	show	VERB
eurjchem-1251	353	8	the	the	DET
eurjchem-1251	353	9	presence	presence	NOUN
eurjchem-1251	353	10	of	of	ADP
eurjchem-1251	353	11	ester	ester	NOUN
eurjchem-1251	353	12	carbonyl	carbonyl	NOUN
eurjchem-1251	353	13	group	group	NOUN
eurjchem-1251	353	14	at	at	ADP
eurjchem-1251	353	15	1718	1718	NUM
eurjchem-1251	353	16	cm‐1	cm‐1	NOUN
eurjchem-1251	353	17	,	,	PUNCT
eurjchem-1251	353	18	c	c	NOUN
eurjchem-1251	353	19	=	=	SYM
eurjchem-1251	353	20	n	n	NOUN
eurjchem-1251	353	21	imino	imino	NOUN
eurjchem-1251	353	22	group	group	NOUN
eurjchem-1251	353	23	at	at	ADP
eurjchem-1251	353	24	1650	1650	NUM
eurjchem-1251	353	25	cm‐1	cm‐1	NOUN
eurjchem-1251	353	26	,	,	PUNCT
eurjchem-1251	353	27	and	and	CCONJ
eurjchem-1251	353	28	the	the	DET
eurjchem-1251	353	29	disappearance	disappearance	NOUN
eurjchem-1251	353	30	of	of	ADP
eurjchem-1251	353	31	the	the	DET
eurjchem-1251	353	32	nh2	nh2	NOUN
eurjchem-1251	353	33	bands	band	NOUN
eurjchem-1251	353	34	.	.	PUNCT
eurjchem-1251	354	1	the	the	DET
eurjchem-1251	354	2	mass	mass	PROPN
eurjchem-1251	354	3	spectrum	spectrum	NOUN
eurjchem-1251	354	4	showed	show	VERB
eurjchem-1251	354	5	the	the	DET
eurjchem-1251	354	6	molecular	molecular	ADJ
eurjchem-1251	354	7	ion	ion	NOUN
eurjchem-1251	354	8	peak	peak	NOUN
eurjchem-1251	354	9	m+	m+	NUM
eurjchem-1251	354	10	at	at	ADP
eurjchem-1251	354	11	m	m	PROPN
eurjchem-1251	354	12	/	/	SYM
eurjchem-1251	354	13	z435	z435	PROPN
eurjchem-1251	354	14	.	.	PUNCT
eurjchem-1251	354	15	further	further	ADJ
eurjchem-1251	354	16	evidence	evidence	NOUN
eurjchem-1251	354	17	for	for	ADP
eurjchem-1251	354	18	the	the	DET
eurjchem-1251	354	19	structure	structure	NOUN
eurjchem-1251	354	20	of	of	ADP
eurjchem-1251	354	21	compound	compound	NOUN
eurjchem-1251	354	22	12a	12a	NOUN
eurjchem-1251	354	23	was	be	AUX
eurjchem-1251	354	24	obtained	obtain	VERB
eurjchem-1251	354	25	by	by	ADP
eurjchem-1251	354	26	hydrolysis	hydrolysis	NOUN
eurjchem-1251	354	27	of	of	ADP
eurjchem-1251	354	28	the	the	DET
eurjchem-1251	354	29	latter	latter	ADJ
eurjchem-1251	354	30	compound	compound	NOUN
eurjchem-1251	354	31	in	in	ADP
eurjchem-1251	354	32	boiling	boil	VERB
eurjchem-1251	354	33	ethanolic	ethanolic	ADJ
eurjchem-1251	354	34	potassium	potassium	NOUN
eurjchem-1251	354	35	hydroxide	hydroxide	NOUN
eurjchem-1251	354	36	to	to	PART
eurjchem-1251	354	37	yield	yield	VERB
eurjchem-1251	354	38	the	the	DET
eurjchem-1251	354	39	corresponding	corresponding	ADJ
eurjchem-1251	354	40	carboxylic	carboxylic	ADJ
eurjchem-1251	354	41	acid	acid	NOUN
eurjchem-1251	354	42	12b	12b	NOUN
eurjchem-1251	354	43	.	.	PUNCT
eurjchem-1251	355	1	however	however	ADV
eurjchem-1251	355	2	,	,	PUNCT
eurjchem-1251	355	3	fusion	fusion	NOUN
eurjchem-1251	355	4	of	of	ADP
eurjchem-1251	355	5	compound	compound	NOUN
eurjchem-1251	355	6	5	5	NUM
eurjchem-1251	355	7	with	with	ADP
eurjchem-1251	355	8	ethyl	ethyl	PROPN
eurjchem-1251	355	9	benzoylacetate	benzoylacetate	NOUN
eurjchem-1251	355	10	produced	produce	VERB
eurjchem-1251	355	11	n‐(4,5,6‐	n‐(4,5,6‐	ADJ
eurjchem-1251	355	12	triphenylpyridazin‐3‐yl)benzoylacetamide	triphenylpyridazin‐3‐yl)benzoylacetamide	NOUN
eurjchem-1251	355	13	,	,	PUNCT
eurjchem-1251	355	14	13	13	NUM
eurjchem-1251	355	15	(	(	PUNCT
eurjchem-1251	355	16	scheme	scheme	NOUN
eurjchem-1251	355	17	3	3	NUM
eurjchem-1251	355	18	)	)	PUNCT
eurjchem-1251	355	19	,	,	PUNCT
eurjchem-1251	355	20	as	as	SCONJ
eurjchem-1251	355	21	proved	prove	VERB
eurjchem-1251	355	22	by	by	ADP
eurjchem-1251	355	23	ir	ir	PROPN
eurjchem-1251	355	24	spectrum	spectrum	NOUN
eurjchem-1251	355	25	showing	show	VERB
eurjchem-1251	355	26	absorption	absorption	NOUN
eurjchem-1251	355	27	bands	band	NOUN
eurjchem-1251	355	28	at	at	ADP
eurjchem-1251	355	29	3429	3429	NUM
eurjchem-1251	355	30	(	(	PUNCT
eurjchem-1251	355	31	nh	nh	PROPN
eurjchem-1251	355	32	,	,	PUNCT
eurjchem-1251	355	33	amide	amide	NOUN
eurjchem-1251	355	34	)	)	PUNCT
eurjchem-1251	355	35	,	,	PUNCT
eurjchem-1251	355	36	1723(c	1723(c	PUNCT
eurjchem-1251	356	1	=	=	SYM
eurjchem-1251	356	2	o	o	NOUN
eurjchem-1251	356	3	,	,	PUNCT
eurjchem-1251	356	4	ketone	ketone	NOUN
eurjchem-1251	356	5	)	)	PUNCT
eurjchem-1251	356	6	and	and	CCONJ
eurjchem-1251	356	7	1677	1677	NUM
eurjchem-1251	356	8	cm‐1	cm‐1	NOUN
eurjchem-1251	356	9	(	(	PUNCT
eurjchem-1251	357	1	c	c	NOUN
eurjchem-1251	357	2	=	=	SYM
eurjchem-1251	357	3	o	o	NOUN
eurjchem-1251	357	4	,	,	PUNCT
eurjchem-1251	357	5	amide	amide	NOUN
eurjchem-1251	357	6	)	)	PUNCT
eurjchem-1251	357	7	.	.	PUNCT
eurjchem-1251	358	1	the	the	DET
eurjchem-1251	358	2	mass	mass	PROPN
eurjchem-1251	358	3	spectrum	spectrum	NOUN
eurjchem-1251	358	4	revealed	reveal	VERB
eurjchem-1251	358	5	the	the	DET
eurjchem-1251	358	6	molecular	molecular	ADJ
eurjchem-1251	358	7	ion	ion	NOUN
eurjchem-1251	358	8	peak	peak	NOUN
eurjchem-1251	358	9	m+	m+	NUM
eurjchem-1251	358	10	at	at	ADP
eurjchem-1251	358	11	m	m	PROPN
eurjchem-1251	358	12	/	/	SYM
eurjchem-1251	358	13	z469.the	z469.the	DET
eurjchem-1251	358	14	study	study	NOUN
eurjchem-1251	358	15	was	be	AUX
eurjchem-1251	358	16	also	also	ADV
eurjchem-1251	358	17	extended	extend	VERB
eurjchem-1251	358	18	to	to	PART
eurjchem-1251	358	19	prepare	prepare	VERB
eurjchem-1251	358	20	some	some	DET
eurjchem-1251	358	21	sulfonamide	sulfonamide	ADJ
eurjchem-1251	358	22	derivatives	derivative	NOUN
eurjchem-1251	358	23	containing	contain	VERB
eurjchem-1251	358	24	the	the	DET
eurjchem-1251	358	25	pyridazine	pyridazine	NOUN
eurjchem-1251	358	26	nucleus	nucleus	NOUN
eurjchem-1251	358	27	with	with	ADP
eurjchem-1251	358	28	the	the	DET
eurjchem-1251	358	29	aim	aim	NOUN
eurjchem-1251	358	30	to	to	PART
eurjchem-1251	358	31	compare	compare	VERB
eurjchem-1251	358	32	the	the	DET
eurjchem-1251	358	33	antimicrobial	antimicrobial	ADJ
eurjchem-1251	358	34	activity	activity	NOUN
eurjchem-1251	358	35	relative	relative	ADJ
eurjchem-1251	358	36	to	to	ADP
eurjchem-1251	358	37	the	the	DET
eurjchem-1251	358	38	systems	system	NOUN
eurjchem-1251	358	39	prepared	prepare	VERB
eurjchem-1251	358	40	earlier	early	ADV
eurjchem-1251	358	41	[	[	X
eurjchem-1251	358	42	18	18	NUM
eurjchem-1251	358	43	]	]	PUNCT
eurjchem-1251	358	44	.	.	PUNCT
eurjchem-1251	359	1	when	when	SCONJ
eurjchem-1251	359	2	3‐chloropyridazine	3‐chloropyridazine	NUM
eurjchem-1251	359	3	derivative	derivative	ADJ
eurjchem-1251	359	4	2	2	NUM
eurjchem-1251	359	5	reacted	react	VERB
eurjchem-1251	359	6	with	with	ADP
eurjchem-1251	359	7	n1‐unsubstituted	n1‐unsubstituted	ADJ
eurjchem-1251	359	8	4‐aminobenzene	4‐aminobenzene	PROPN
eurjchem-1251	359	9	sulfonamides	sulfonamide	NOUN
eurjchem-1251	359	10	14a	14a	NOUN
eurjchem-1251	359	11	,	,	PUNCT
eurjchem-1251	359	12	and	and	CCONJ
eurjchem-1251	359	13	n	n	PROPN
eurjchem-1251	359	14	1‐substituted	1‐substituted	NUM
eurjchem-1251	359	15	4‐aminobenzenesulfon	4‐aminobenzenesulfon	PROPN
eurjchem-1251	359	16	amides	amide	NOUN
eurjchem-1251	359	17	14b‐g	14b‐g	NOUN
eurjchem-1251	359	18	,	,	PUNCT
eurjchem-1251	359	19	n1‐4‐[(4	n1‐4‐[(4	PROPN
eurjchem-1251	359	20	,	,	PUNCT
eurjchem-1251	359	21	5	5	NUM
eurjchem-1251	359	22	,	,	PUNCT
eurjchem-1251	359	23	6‐triphenylpyridzin‐3‐yl)amino	6‐triphenylpyridzin‐3‐yl)amino	NUM
eurjchem-1251	359	24	]	]	X
eurjchem-1251	359	25	benzenesulfonamide	benzenesulfonamide	NOUN
eurjchem-1251	359	26	,	,	PUNCT
eurjchem-1251	359	27	15a‐g	15a‐g	NOUN
eurjchem-1251	359	28	were	be	AUX
eurjchem-1251	359	29	produced	produce	VERB
eurjchem-1251	359	30	(	(	PUNCT
eurjchem-1251	359	31	scheme	scheme	NOUN
eurjchem-1251	359	32	4	4	NUM
eurjchem-1251	359	33	)	)	PUNCT
eurjchem-1251	359	34	.	.	PUNCT
eurjchem-1251	360	1	the	the	DET
eurjchem-1251	360	2	structure	structure	NOUN
eurjchem-1251	360	3	of	of	ADP
eurjchem-1251	360	4	the	the	DET
eurjchem-1251	360	5	latter	latter	ADJ
eurjchem-1251	360	6	compounds	compound	NOUN
eurjchem-1251	360	7	was	be	AUX
eurjchem-1251	360	8	established	establish	VERB
eurjchem-1251	360	9	on	on	ADP
eurjchem-1251	360	10	the	the	DET
eurjchem-1251	360	11	basis	basis	NOUN
eurjchem-1251	360	12	of	of	ADP
eurjchem-1251	360	13	elemental	elemental	ADJ
eurjchem-1251	360	14	analysis	analysis	NOUN
eurjchem-1251	360	15	,	,	PUNCT
eurjchem-1251	360	16	ir	ir	PROPN
eurjchem-1251	360	17	,	,	PUNCT
eurjchem-1251	360	18	mass	mass	PROPN
eurjchem-1251	360	19	,	,	PUNCT
eurjchem-1251	360	20	1h	1h	NUM
eurjchem-1251	360	21	nmr	nmr	PROPN
eurjchem-1251	360	22	spectra	spectra	PROPN
eurjchem-1251	360	23	.	.	PUNCT
eurjchem-1251	361	1	the	the	DET
eurjchem-1251	361	2	sulfonamide	sulfonamide	NOUN
eurjchem-1251	361	3	derivatives	derivative	NOUN
eurjchem-1251	361	4	14a‐g	14a‐g	NOUN
eurjchem-1251	361	5	was	be	AUX
eurjchem-1251	361	6	prepared	prepare	VERB
eurjchem-1251	361	7	using	use	VERB
eurjchem-1251	361	8	a	a	DET
eurjchem-1251	361	9	previously	previously	ADV
eurjchem-1251	361	10	described	describe	VERB
eurjchem-1251	361	11	method	method	NOUN
eurjchem-1251	361	12	[	[	X
eurjchem-1251	361	13	19	19	NUM
eurjchem-1251	361	14	]	]	PUNCT
eurjchem-1251	361	15	.	.	PUNCT
eurjchem-1251	362	1	3.2	3.2	NUM
eurjchem-1251	362	2	.	.	PUNCT
eurjchem-1251	362	3	antimicrobial	antimicrobial	ADJ
eurjchem-1251	362	4	activity	activity	NOUN
eurjchem-1251	362	5	bioassay	bioassay	VERB
eurjchem-1251	362	6	the	the	DET
eurjchem-1251	362	7	results	result	NOUN
eurjchem-1251	362	8	(	(	PUNCT
eurjchem-1251	362	9	table	table	NOUN
eurjchem-1251	362	10	1	1	NUM
eurjchem-1251	362	11	)	)	PUNCT
eurjchem-1251	362	12	indicated	indicate	VERB
eurjchem-1251	362	13	that	that	SCONJ
eurjchem-1251	362	14	two	two	NUM
eurjchem-1251	362	15	synthesized	synthesize	VERB
eurjchem-1251	362	16	compounds	compound	NOUN
eurjchem-1251	362	17	5	5	NUM
eurjchem-1251	362	18	and	and	CCONJ
eurjchem-1251	362	19	15ginhibited	15ginhibited	NUM
eurjchem-1251	362	20	the	the	DET
eurjchem-1251	362	21	growth	growth	NOUN
eurjchem-1251	362	22	of	of	ADP
eurjchem-1251	362	23	the	the	DET
eurjchem-1251	362	24	gram	gram	PROPN
eurjchem-1251	362	25	positive	positive	ADJ
eurjchem-1251	362	26	bacteria	bacteria	NOUN
eurjchem-1251	362	27	staphylococcus	staphylococcus	NOUN
eurjchem-1251	362	28	aureus	aureus	NOUN
eurjchem-1251	362	29	completely	completely	ADV
eurjchem-1251	362	30	,	,	PUNCT
eurjchem-1251	362	31	while	while	SCONJ
eurjchem-1251	362	32	compound	compound	NOUN
eurjchem-1251	362	33	15e	15e	NOUN
eurjchem-1251	362	34	showed	show	VERB
eurjchem-1251	362	35	relatively	relatively	ADV
eurjchem-1251	362	36	very	very	ADV
eurjchem-1251	362	37	high	high	ADJ
eurjchem-1251	362	38	antimicrobial	antimicrobial	ADJ
eurjchem-1251	362	39	activity	activity	NOUN
eurjchem-1251	362	40	against	against	ADP
eurjchem-1251	362	41	bacillus	bacillus	NOUN
eurjchem-1251	362	42	subtilis	subtili	NOUN
eurjchem-1251	362	43	.	.	PUNCT
eurjchem-1251	363	1	on	on	ADP
eurjchem-1251	363	2	the	the	DET
eurjchem-1251	363	3	other	other	ADJ
eurjchem-1251	363	4	hand	hand	NOUN
eurjchem-1251	363	5	,	,	PUNCT
eurjchem-1251	363	6	the	the	DET
eurjchem-1251	363	7	latter	latter	ADJ
eurjchem-1251	363	8	compound	compound	NOUN
eurjchem-1251	363	9	15e	15e	NOUN
eurjchem-1251	363	10	;	;	PUNCT
eurjchem-1251	363	11	as	as	ADV
eurjchem-1251	363	12	well	well	ADV
eurjchem-1251	363	13	as	as	ADP
eurjchem-1251	363	14	compounds	compound	NOUN
eurjchem-1251	363	15	15d	15d	NOUN
eurjchem-1251	363	16	and	and	CCONJ
eurjchem-1251	363	17	15f	15f	PROPN
eurjchem-1251	363	18	showed	show	VERB
eurjchem-1251	363	19	high	high	ADJ
eurjchem-1251	363	20	activity	activity	NOUN
eurjchem-1251	363	21	against	against	ADP
eurjchem-1251	363	22	both	both	DET
eurjchem-1251	363	23	staphylococcus	staphylococcus	NOUN
eurjchem-1251	363	24	aureus	aureus	NOUN
eurjchem-1251	363	25	and	and	CCONJ
eurjchem-1251	363	26	bacillus	bacillus	NOUN
eurjchem-1251	363	27	subtilis	subtili	NOUN
eurjchem-1251	363	28	,	,	PUNCT
eurjchem-1251	363	29	respectively	respectively	ADV
eurjchem-1251	363	30	.	.	PUNCT
eurjchem-1251	364	1	compounds	compound	VERB
eurjchem-1251	364	2	9	9	NUM
eurjchem-1251	364	3	,	,	PUNCT
eurjchem-1251	364	4	11a	11a	NOUN
eurjchem-1251	364	5	,	,	PUNCT
eurjchem-1251	364	6	15a	15a	NOUN
eurjchem-1251	364	7	,	,	PUNCT
eurjchem-1251	364	8	15b	15b	NOUN
eurjchem-1251	364	9	,	,	PUNCT
eurjchem-1251	364	10	15c	15c	NOUN
eurjchem-1251	364	11	and	and	CCONJ
eurjchem-1251	364	12	15d	15d	NUM
eurjchem-1251	364	13	possessed	possess	VERB
eurjchem-1251	364	14	moderate	moderate	ADJ
eurjchem-1251	364	15	activity	activity	NOUN
eurjchem-1251	364	16	against	against	ADP
eurjchem-1251	364	17	staphylococcus	staphylococcus	NOUN
eurjchem-1251	364	18	aureus	aureus	NOUN
eurjchem-1251	364	19	,	,	PUNCT
eurjchem-1251	364	20	while	while	SCONJ
eurjchem-1251	364	21	compounds	compound	NOUN
eurjchem-1251	364	22	9	9	NUM
eurjchem-1251	364	23	,	,	PUNCT
eurjchem-1251	364	24	11a	11a	NOUN
eurjchem-1251	364	25	,	,	PUNCT
eurjchem-1251	364	26	15c	15c	NOUN
eurjchem-1251	364	27	and	and	CCONJ
eurjchem-1251	364	28	15	15	NUM
eurjchem-1251	364	29	g	g	NOUN
eurjchem-1251	364	30	showed	show	VERB
eurjchem-1251	364	31	moderate	moderate	ADJ
eurjchem-1251	364	32	inhibition	inhibition	NOUN
eurjchem-1251	364	33	of	of	ADP
eurjchem-1251	364	34	bacillus	bacillus	NOUN
eurjchem-1251	364	35	subtilis	subtili	NOUN
eurjchem-1251	364	36	.	.	PUNCT
eurjchem-1251	365	1	only	only	ADV
eurjchem-1251	365	2	compounds	compound	NOUN
eurjchem-1251	365	3	9	9	NUM
eurjchem-1251	365	4	,	,	PUNCT
eurjchem-1251	365	5	11a	11a	NOUN
eurjchem-1251	365	6	and	and	CCONJ
eurjchem-1251	365	7	15c	15c	NOUN
eurjchem-1251	365	8	showed	show	VERB
eurjchem-1251	365	9	moderate	moderate	ADJ
eurjchem-1251	365	10	antimicrobial	antimicrobial	ADJ
eurjchem-1251	365	11	activity	activity	NOUN
eurjchem-1251	365	12	against	against	ADP
eurjchem-1251	365	13	both	both	DET
eurjchem-1251	365	14	examined	examine	VERB
eurjchem-1251	365	15	staphylococcus	staphylococcus	NOUN
eurjchem-1251	365	16	aureus	aureus	NOUN
eurjchem-1251	365	17	and	and	CCONJ
eurjchem-1251	365	18	bacillus	bacillus	NOUN
eurjchem-1251	365	19	subtilis	subtili	NOUN
eurjchem-1251	365	20	.	.	PUNCT
eurjchem-1251	366	1	on	on	ADP
eurjchem-1251	366	2	the	the	DET
eurjchem-1251	366	3	other	other	ADJ
eurjchem-1251	366	4	hand	hand	NOUN
eurjchem-1251	366	5	,	,	PUNCT
eurjchem-1251	366	6	compound	compound	NOUN
eurjchem-1251	366	7	11a	11a	NOUN
eurjchem-1251	366	8	showed	show	VERB
eurjchem-1251	366	9	relatively	relatively	ADV
eurjchem-1251	366	10	very	very	ADV
eurjchem-1251	366	11	high	high	ADJ
eurjchem-1251	366	12	antimicrobial	antimicrobial	ADJ
eurjchem-1251	366	13	activity	activity	NOUN
eurjchem-1251	366	14	against	against	ADP
eurjchem-1251	366	15	escherichia	escherichia	NOUN
eurjchem-1251	366	16	coli	coli	NOUN
eurjchem-1251	366	17	.	.	PUNCT
eurjchem-1251	367	1	in	in	ADP
eurjchem-1251	367	2	addition	addition	NOUN
eurjchem-1251	367	3	,	,	PUNCT
eurjchem-1251	367	4	compounds	compound	VERB
eurjchem-1251	367	5	9	9	NUM
eurjchem-1251	367	6	,	,	PUNCT
eurjchem-1251	367	7	15b	15b	NUM
eurjchem-1251	367	8	,	,	PUNCT
eurjchem-1251	367	9	15d	15d	NUM
eurjchem-1251	367	10	and	and	CCONJ
eurjchem-1251	367	11	15f	15f	NOUN
eurjchem-1251	367	12	;	;	PUNCT
eurjchem-1251	367	13	and	and	CCONJ
eurjchem-1251	367	14	compounds	compound	VERB
eurjchem-1251	367	15	6b	6b	NOUN
eurjchem-1251	367	16	,	,	PUNCT
eurjchem-1251	367	17	9	9	NUM
eurjchem-1251	367	18	,	,	PUNCT
eurjchem-1251	367	19	11a	11a	NOUN
eurjchem-1251	367	20	and	and	CCONJ
eurjchem-1251	367	21	15e	15e	NOUN
eurjchem-1251	367	22	possessed	possess	VERB
eurjchem-1251	367	23	high	high	ADJ
eurjchem-1251	367	24	activity	activity	NOUN
eurjchem-1251	367	25	against	against	ADP
eurjchem-1251	367	26	escherichia	escherichia	NOUN
eurjchem-1251	367	27	coli	coli	NOUN
eurjchem-1251	367	28	and	and	CCONJ
eurjchem-1251	367	29	pseudomonas	pseudomona	NOUN
eurjchem-1251	367	30	aeruginosa	aeruginosa	NOUN
eurjchem-1251	367	31	,	,	PUNCT
eurjchem-1251	367	32	respectively	respectively	ADV
eurjchem-1251	367	33	.	.	PUNCT
eurjchem-1251	368	1	compound	compound	NOUN
eurjchem-1251	368	2	9	9	NUM
eurjchem-1251	368	3	was	be	AUX
eurjchem-1251	368	4	highlyactive	highlyactive	ADJ
eurjchem-1251	368	5	against	against	ADP
eurjchem-1251	368	6	both	both	DET
eurjchem-1251	368	7	escherichia	escherichia	NOUN
eurjchem-1251	368	8	coli	coli	NOUN
eurjchem-1251	368	9	and	and	CCONJ
eurjchem-1251	368	10	pseudomonas	pseudomona	NOUN
eurjchem-1251	368	11	aeruginosa	aeruginosa	NOUN
eurjchem-1251	368	12	.	.	PUNCT
eurjchem-1251	369	1	also	also	ADV
eurjchem-1251	369	2	,	,	PUNCT
eurjchem-1251	369	3	the	the	DET
eurjchem-1251	369	4	results	result	NOUN
eurjchem-1251	369	5	indicated	indicate	VERB
eurjchem-1251	369	6	thatcompounds	thatcompound	NOUN
eurjchem-1251	369	7	5	5	NUM
eurjchem-1251	369	8	,	,	PUNCT
eurjchem-1251	369	9	6b	6b	NOUN
eurjchem-1251	369	10	,	,	PUNCT
eurjchem-1251	369	11	15e	15e	NOUN
eurjchem-1251	369	12	and	and	CCONJ
eurjchem-1251	369	13	15	15	NUM
eurjchem-1251	369	14	g	g	NOUN
eurjchem-1251	369	15	;	;	PUNCT
eurjchem-1251	369	16	and	and	CCONJ
eurjchem-1251	369	17	compounds	compound	VERB
eurjchem-1251	369	18	5	5	NUM
eurjchem-1251	369	19	,	,	PUNCT
eurjchem-1251	369	20	15b	15b	NUM
eurjchem-1251	369	21	,	,	PUNCT
eurjchem-1251	369	22	15c	15c	NOUN
eurjchem-1251	369	23	,	,	PUNCT
eurjchem-1251	369	24	15d	15d	NUM
eurjchem-1251	369	25	,	,	PUNCT
eurjchem-1251	369	26	15f	15f	PROPN
eurjchem-1251	369	27	and	and	CCONJ
eurjchem-1251	369	28	15	15	NUM
eurjchem-1251	369	29	g	g	NOUN
eurjchem-1251	369	30	showed	show	VERB
eurjchem-1251	369	31	moderate	moderate	ADJ
eurjchem-1251	369	32	activity	activity	NOUN
eurjchem-1251	369	33	against	against	ADP
eurjchem-1251	369	34	escherichia	escherichia	NOUN
eurjchem-1251	369	35	coli	coli	NOUN
eurjchem-1251	369	36	and	and	CCONJ
eurjchem-1251	369	37	pseudomonas	pseudomona	NOUN
eurjchem-1251	369	38	aeruginosa	aeruginosa	NOUN
eurjchem-1251	369	39	,	,	PUNCT
eurjchem-1251	369	40	respectively	respectively	ADV
eurjchem-1251	369	41	.	.	PUNCT
eurjchem-1251	370	1	compounds	compound	VERB
eurjchem-1251	370	2	5	5	NUM
eurjchem-1251	370	3	and	and	CCONJ
eurjchem-1251	370	4	15	15	NUM
eurjchem-1251	370	5	g	g	NOUN
eurjchem-1251	370	6	were	be	AUX
eurjchem-1251	370	7	moderate	moderate	ADJ
eurjchem-1251	370	8	active	active	ADJ
eurjchem-1251	370	9	against	against	ADP
eurjchem-1251	370	10	both	both	DET
eurjchem-1251	370	11	escherichia	escherichia	NOUN
eurjchem-1251	370	12	coli	coli	NOUN
eurjchem-1251	370	13	and	and	CCONJ
eurjchem-1251	370	14	pseudomonas	pseudomona	NOUN
eurjchem-1251	370	15	aeruginosa	aeruginosa	NOUN
eurjchem-1251	370	16	.	.	PUNCT
eurjchem-1251	371	1	the	the	DET
eurjchem-1251	371	2	results	result	NOUN
eurjchem-1251	371	3	revealed	reveal	VERB
eurjchem-1251	371	4	that	that	SCONJ
eurjchem-1251	371	5	compounds	compound	VERB
eurjchem-1251	371	6	15c	15c	NOUN
eurjchem-1251	371	7	,	,	PUNCT
eurjchem-1251	371	8	15d	15d	NUM
eurjchem-1251	371	9	and	and	CCONJ
eurjchem-1251	371	10	15f	15f	PROPN
eurjchem-1251	371	11	showed	show	VERB
eurjchem-1251	371	12	complete	complete	ADJ
eurjchem-1251	371	13	inhibition	inhibition	NOUN
eurjchem-1251	371	14	for	for	ADP
eurjchem-1251	371	15	the	the	DET
eurjchem-1251	371	16	growth	growth	NOUN
eurjchem-1251	371	17	of	of	ADP
eurjchem-1251	371	18	aspergillus	aspergillus	NOUN
eurjchem-1251	371	19	niger	niger	NOUN
eurjchem-1251	371	20	.	.	PUNCT
eurjchem-1251	372	1	in	in	ADP
eurjchem-1251	372	2	addition	addition	NOUN
eurjchem-1251	372	3	,	,	PUNCT
eurjchem-1251	372	4	compound	compound	NOUN
eurjchem-1251	372	5	15c	15c	NOUN
eurjchem-1251	372	6	;	;	PUNCT
eurjchem-1251	372	7	as	as	ADV
eurjchem-1251	372	8	well	well	ADV
eurjchem-1251	372	9	as	as	ADP
eurjchem-1251	372	10	compounds	compound	NOUN
eurjchem-1251	372	11	9	9	NUM
eurjchem-1251	372	12	,	,	PUNCT
eurjchem-1251	372	13	11a	11a	NOUN
eurjchem-1251	372	14	,	,	PUNCT
eurjchem-1251	372	15	15a	15a	NOUN
eurjchem-1251	372	16	and	and	CCONJ
eurjchem-1251	372	17	15b	15b	NOUN
eurjchem-1251	372	18	were	be	AUX
eurjchem-1251	372	19	highly	highly	ADV
eurjchem-1251	372	20	active	active	ADJ
eurjchem-1251	372	21	against	against	ADP
eurjchem-1251	372	22	candida	candida	NOUN
eurjchem-1251	372	23	albicans	albican	NOUN
eurjchem-1251	372	24	and	and	CCONJ
eurjchem-1251	372	25	aspergillus	aspergillus	NOUN
eurjchem-1251	372	26	niger	niger	NOUN
eurjchem-1251	372	27	,	,	PUNCT
eurjchem-1251	372	28	respectively	respectively	ADV
eurjchem-1251	372	29	.	.	PUNCT
eurjchem-1251	373	1	also	also	ADV
eurjchem-1251	373	2	,	,	PUNCT
eurjchem-1251	373	3	the	the	DET
eurjchem-1251	373	4	results	result	NOUN
eurjchem-1251	373	5	indicatedthat	indicatedthat	PRON
eurjchem-1251	373	6	compounds	compound	VERB
eurjchem-1251	373	7	6b	6b	NOUN
eurjchem-1251	373	8	,	,	PUNCT
eurjchem-1251	373	9	9	9	NUM
eurjchem-1251	373	10	,	,	PUNCT
eurjchem-1251	373	11	11a	11a	NOUN
eurjchem-1251	373	12	,	,	PUNCT
eurjchem-1251	373	13	15a	15a	NOUN
eurjchem-1251	373	14	,	,	PUNCT
eurjchem-1251	373	15	15b	15b	NOUN
eurjchem-1251	373	16	,	,	PUNCT
eurjchem-1251	373	17	15d	15d	NUM
eurjchem-1251	373	18	and	and	CCONJ
eurjchem-1251	373	19	15f	15f	NOUN
eurjchem-1251	373	20	;	;	PUNCT
eurjchem-1251	373	21	as	as	ADV
eurjchem-1251	373	22	well	well	ADV
eurjchem-1251	373	23	as	as	ADP
eurjchem-1251	373	24	compound	compound	NOUN
eurjchem-1251	373	25	6b	6b	NOUN
eurjchem-1251	373	26	showed	show	VERB
eurjchem-1251	373	27	moderate	moderate	ADJ
eurjchem-1251	373	28	activity	activity	NOUN
eurjchem-1251	373	29	against	against	ADP
eurjchem-1251	373	30	candida	candida	NOUN
eurjchem-1251	373	31	albicans	albican	NOUN
eurjchem-1251	373	32	and	and	CCONJ
eurjchem-1251	373	33	aspergillus	aspergillus	NOUN
eurjchem-1251	373	34	niger	niger	NOUN
eurjchem-1251	373	35	,	,	PUNCT
eurjchem-1251	373	36	respectively	respectively	ADV
eurjchem-1251	373	37	.	.	PUNCT
eurjchem-1251	374	1	compound	compound	NOUN
eurjchem-1251	374	2	6b	6b	PROPN
eurjchem-1251	374	3	showed	show	VERB
eurjchem-1251	374	4	moderateinhibition	moderateinhibition	NOUN
eurjchem-1251	374	5	of	of	ADP
eurjchem-1251	374	6	both	both	PRON
eurjchem-1251	374	7	candida	candida	NOUN
eurjchem-1251	374	8	albicans	albican	NOUN
eurjchem-1251	374	9	and	and	CCONJ
eurjchem-1251	374	10	aspergillus	aspergillus	NOUN
eurjchem-1251	374	11	niger	niger	NOUN
eurjchem-1251	374	12	.	.	PUNCT
eurjchem-1251	375	1	in	in	ADP
eurjchem-1251	375	2	general	general	ADJ
eurjchem-1251	375	3	,	,	PUNCT
eurjchem-1251	375	4	the	the	DET
eurjchem-1251	375	5	synthesised	synthesise	VERB
eurjchem-1251	375	6	compounds	compound	NOUN
eurjchem-1251	375	7	showed	show	VERB
eurjchem-1251	375	8	moderate	moderate	ADJ
eurjchem-1251	375	9	to	to	ADP
eurjchem-1251	375	10	high	high	ADJ
eurjchem-1251	375	11	antimicrobial	antimicrobial	ADJ
eurjchem-1251	375	12	activity	activity	NOUN
eurjchem-1251	375	13	against	against	ADP
eurjchem-1251	375	14	the	the	DET
eurjchem-1251	375	15	microorganisms	microorganism	NOUN
eurjchem-1251	375	16	under	under	ADP
eurjchem-1251	375	17	test	test	NOUN
eurjchem-1251	375	18	comparable	comparable	ADJ
eurjchem-1251	375	19	with	with	ADP
eurjchem-1251	375	20	the	the	DET
eurjchem-1251	375	21	standard	standard	ADJ
eurjchem-1251	375	22	septrin	septrin	NOUN
eurjchem-1251	375	23	d.s	d.s	PROPN
eurjchem-1251	375	24	.	.	PROPN
eurjchem-1251	375	25	and	and	CCONJ
eurjchem-1251	375	26	fungistatin	fungistatin	NOUN
eurjchem-1251	375	27	.	.	PUNCT
eurjchem-1251	376	1	4	4	X
eurjchem-1251	376	2	.	.	X
eurjchem-1251	376	3	conclusion	conclusion	NOUN
eurjchem-1251	376	4	a	a	DET
eurjchem-1251	376	5	new	new	ADJ
eurjchem-1251	376	6	series	series	NOUN
eurjchem-1251	376	7	of	of	ADP
eurjchem-1251	376	8	aminopyridazine	aminopyridazine	NOUN
eurjchem-1251	376	9	bearing	bear	VERB
eurjchem-1251	376	10	sulfonamide	sulfonamide	ADJ
eurjchem-1251	376	11	moiety	moiety	NOUN
eurjchem-1251	376	12	and	and	CCONJ
eurjchem-1251	376	13	pyrimidopyridazine	pyrimidopyridazine	NOUN
eurjchem-1251	376	14	were	be	AUX
eurjchem-1251	376	15	synthesized	synthesize	VERB
eurjchem-1251	376	16	and	and	CCONJ
eurjchem-1251	376	17	biological	biological	ADJ
eurjchem-1251	376	18	evaluated	evaluate	VERB
eurjchem-1251	376	19	.	.	PUNCT
eurjchem-1251	377	1	compounds	compound	VERB
eurjchem-1251	377	2	5	5	NUM
eurjchem-1251	377	3	and	and	CCONJ
eurjchem-1251	377	4	15a‐g	15a‐g	NOUN
eurjchem-1251	377	5	showed	show	VERB
eurjchem-1251	377	6	promising	promise	VERB
eurjchem-1251	377	7	antibacterial	antibacterial	ADJ
eurjchem-1251	377	8	activities	activity	NOUN
eurjchem-1251	377	9	,	,	PUNCT
eurjchem-1251	377	10	compared	compare	VERB
eurjchem-1251	377	11	with	with	ADP
eurjchem-1251	377	12	the	the	DET
eurjchem-1251	377	13	reference	reference	NOUN
eurjchem-1251	377	14	drugs	drug	NOUN
eurjchem-1251	377	15	.	.	PUNCT
eurjchem-1251	378	1	218	218	NUM
eurjchem-1251	378	2	deeb	deeb	PROPN
eurjchem-1251	378	3	et	et	PROPN
eurjchem-1251	378	4	al	al	PROPN
eurjchem-1251	378	5	.	.	PUNCT
eurjchem-1251	378	6	/	/	SYM
eurjchem-1251	378	7	european	european	PROPN
eurjchem-1251	378	8	journal	journal	PROPN
eurjchem-1251	378	9	of	of	ADP
eurjchem-1251	378	10	chemistry	chemistry	NOUN
eurjchem-1251	378	11	6	6	NUM
eurjchem-1251	378	12	(	(	PUNCT
eurjchem-1251	378	13	2	2	NUM
eurjchem-1251	378	14	)	)	PUNCT
eurjchem-1251	378	15	(	(	PUNCT
eurjchem-1251	378	16	2015	2015	NUM
eurjchem-1251	378	17	)	)	PUNCT
eurjchem-1251	378	18	211‐218	211‐218	NUM
eurjchem-1251	378	19	acknowledgement	acknowledgement	NOUN
eurjchem-1251	378	20	the	the	DET
eurjchem-1251	378	21	author	author	NOUN
eurjchem-1251	378	22	acknowledges	acknowledge	VERB
eurjchem-1251	378	23	the	the	DET
eurjchem-1251	378	24	help	help	NOUN
eurjchem-1251	378	25	of	of	ADP
eurjchem-1251	378	26	prof.dr	prof.dr	PROPN
eurjchem-1251	378	27	.	.	PUNCT
eurjchem-1251	379	1	yeha	yeha	PROPN
eurjchem-1251	379	2	ahmed	ahmed	PROPN
eurjchem-1251	379	3	el‐zawahry	el‐zawahry	PROPN
eurjchem-1251	379	4	,	,	PUNCT
eurjchem-1251	379	5	department	department	NOUN
eurjchem-1251	379	6	of	of	ADP
eurjchem-1251	379	7	microbiology	microbiology	NOUN
eurjchem-1251	379	8	for	for	ADP
eurjchem-1251	379	9	carrying	carry	VERB
eurjchem-1251	379	10	out	out	ADP
eurjchem-1251	379	11	the	the	DET
eurjchem-1251	379	12	antimicrobial	antimicrobial	ADJ
eurjchem-1251	379	13	activity	activity	NOUN
eurjchem-1251	379	14	.	.	PUNCT
eurjchem-1251	380	1	references	reference	NOUN
eurjchem-1251	380	2	[	[	X
eurjchem-1251	380	3	1	1	NUM
eurjchem-1251	380	4	]	]	PUNCT
eurjchem-1251	380	5	.	.	PUNCT
eurjchem-1251	381	1	vandermey	vandermey	PROPN
eurjchem-1251	381	2	,	,	PUNCT
eurjchem-1251	381	3	m.	m.	NOUN
eurjchem-1251	381	4	;	;	PUNCT
eurjchem-1251	381	5	boss	boss	NOUN
eurjchem-1251	381	6	,	,	PUNCT
eurjchem-1251	381	7	h.	h.	PROPN
eurjchem-1251	381	8	;	;	PUNCT
eurjchem-1251	381	9	hatzelmann	hatzelmann	PROPN
eurjchem-1251	381	10	,	,	PUNCT
eurjchem-1251	381	11	a.	a.	NOUN
eurjchem-1251	381	12	;	;	PUNCT
eurjchem-1251	381	13	vanderlaan	vanderlaan	PROPN
eurjchem-1251	381	14	,	,	PUNCT
eurjchem-1251	381	15	i.	i.	PROPN
eurjchem-1251	381	16	j.	j.	PROPN
eurjchem-1251	381	17	;	;	PUNCT
eurjchem-1251	381	18	sterk	sterk	PROPN
eurjchem-1251	381	19	,	,	PUNCT
eurjchem-1251	381	20	g.	g.	PROPN
eurjchem-1251	381	21	i.	i.	PROPN
eurjchem-1251	381	22	;	;	PUNCT
eurjchem-1251	381	23	timmerman	timmerman	PROPN
eurjchem-1251	381	24	,	,	PUNCT
eurjchem-1251	381	25	h.	h.	PROPN
eurjchem-1251	381	26	j.	j.	PROPN
eurjchem-1251	381	27	med	med	PROPN
eurjchem-1251	381	28	.	.	PROPN
eurjchem-1251	381	29	chem	chem	PROPN
eurjchem-1251	381	30	.	.	PUNCT
eurjchem-1251	382	1	2002	2002	NUM
eurjchem-1251	382	2	,	,	PUNCT
eurjchem-1251	382	3	45	45	NUM
eurjchem-1251	382	4	,	,	PUNCT
eurjchem-1251	382	5	2520‐2523	2520‐2523	NUM
eurjchem-1251	382	6	.	.	PUNCT
eurjchem-1251	383	1	[	[	X
eurjchem-1251	383	2	2	2	NUM
eurjchem-1251	383	3	]	]	PUNCT
eurjchem-1251	383	4	.	.	PUNCT
eurjchem-1251	383	5	bradbury	bradbury	PROPN
eurjchem-1251	383	6	,	,	PUNCT
eurjchem-1251	383	7	r.	r.	PROPN
eurjchem-1251	383	8	h.	h.	PROPN
eurjchem-1251	383	9	;	;	PUNCT
eurjchem-1251	383	10	bath	bath	NOUN
eurjchem-1251	383	11	,	,	PUNCT
eurjchem-1251	383	12	c.	c.	PROPN
eurjchem-1251	383	13	;	;	PUNCT
eurjchem-1251	383	14	butlin	butlin	PROPN
eurjchem-1251	383	15	,	,	PUNCT
eurjchem-1251	383	16	r.	r.	PROPN
eurjchem-1251	383	17	j.	j.	PROPN
eurjchem-1251	383	18	;	;	PUNCT
eurjchem-1251	383	19	dennis	dennis	PROPN
eurjchem-1251	383	20	,	,	PUNCT
eurjchem-1251	383	21	m.	m.	NOUN
eurjchem-1251	383	22	;	;	PUNCT
eurjchem-1251	383	23	heys	heys	PROPN
eurjchem-1251	383	24	,	,	PUNCT
eurjchem-1251	383	25	c.	c.	PROPN
eurjchem-1251	383	26	;	;	PUNCT
eurjchem-1251	383	27	hunt	hunt	PROPN
eurjchem-1251	383	28	,	,	PUNCT
eurjchem-1251	383	29	s.	s.	PROPN
eurjchem-1251	383	30	j.	j.	PROPN
eurjchem-1251	383	31	;	;	PUNCT
eurjchem-1251	383	32	james	james	PROPN
eurjchem-1251	383	33	,	,	PUNCT
eurjchem-1251	383	34	r.	r.	PROPN
eurjchem-1251	383	35	;	;	PUNCT
eurjchem-1251	383	36	mortlock	mortlock	NOUN
eurjchem-1251	383	37	,	,	PUNCT
eurjchem-1251	383	38	a.	a.	NOUN
eurjchem-1251	383	39	a.	a.	NOUN
eurjchem-1251	383	40	;	;	PUNCT
eurjchem-1251	383	41	sumner	sumner	PROPN
eurjchem-1251	383	42	,	,	PUNCT
eurjchem-1251	383	43	n.	n.	PROPN
eurjchem-1251	383	44	f.	f.	PROPN
eurjchem-1251	383	45	;	;	PUNCT
eurjchem-1251	383	46	tang	tang	PROPN
eurjchem-1251	383	47	,	,	PUNCT
eurjchem-1251	383	48	e.	e.	PROPN
eurjchem-1251	383	49	k.	k.	PROPN
eurjchem-1251	383	50	;	;	PUNCT
eurjchem-1251	383	51	telford	telford	PROPN
eurjchem-1251	383	52	,	,	PUNCT
eurjchem-1251	383	53	b.	b.	PROPN
eurjchem-1251	383	54	;	;	PUNCT
eurjchem-1251	383	55	whiting	whiting	NOUN
eurjchem-1251	383	56	,	,	PUNCT
eurjchem-1251	383	57	e.	e.	PROPN
eurjchem-1251	383	58	;	;	PUNCT
eurjchem-1251	383	59	wilson	wilson	PROPN
eurjchem-1251	383	60	,	,	PUNCT
eurjchem-1251	383	61	c.	c.	PROPN
eurjchem-1251	383	62	j.	j.	PROPN
eurjchem-1251	383	63	med	med	PROPN
eurjchem-1251	383	64	.	.	PROPN
eurjchem-1251	383	65	chem	chem	PROPN
eurjchem-1251	383	66	.	.	PUNCT
eurjchem-1251	384	1	1997	1997	NUM
eurjchem-1251	384	2	,	,	PUNCT
eurjchem-1251	384	3	40	40	NUM
eurjchem-1251	384	4	,	,	PUNCT
eurjchem-1251	384	5	996‐1004	996‐1004	NUM
eurjchem-1251	384	6	.	.	PUNCT
eurjchem-1251	385	1	[	[	X
eurjchem-1251	385	2	3	3	NUM
eurjchem-1251	385	3	]	]	PUNCT
eurjchem-1251	385	4	.	.	PUNCT
eurjchem-1251	386	1	barbara	barbara	PROPN
eurjchem-1251	386	2	,	,	PUNCT
eurjchem-1251	386	3	r.	r.	PROPN
eurjchem-1251	386	4	;	;	PUNCT
eurjchem-1251	386	5	betti	betti	PROPN
eurjchem-1251	386	6	,	,	PUNCT
eurjchem-1251	386	7	l.	l.	PROPN
eurjchem-1251	386	8	;	;	PUNCT
eurjchem-1251	386	9	botta	botta	PROPN
eurjchem-1251	386	10	,	,	PUNCT
eurjchem-1251	386	11	m.	m.	NOUN
eurjchem-1251	386	12	;	;	PUNCT
eurjchem-1251	386	13	corelli	corelli	PROPN
eurjchem-1251	386	14	,	,	PUNCT
eurjchem-1251	386	15	f.	f.	PROPN
eurjchem-1251	386	16	;	;	PUNCT
eurjchem-1251	386	17	giannaccini	giannaccini	PROPN
eurjchem-1251	386	18	,	,	PUNCT
eurjchem-1251	386	19	g.	g.	PROPN
eurjchem-1251	386	20	;	;	PUNCT
eurjchem-1251	386	21	maccari	maccari	PROPN
eurjchem-1251	386	22	,	,	PUNCT
eurjchem-1251	386	23	l.	l.	PROPN
eurjchem-1251	386	24	;	;	PUNCT
eurjchem-1251	386	25	manetti	manetti	PROPN
eurjchem-1251	386	26	,	,	PUNCT
eurjchem-1251	386	27	f.	f.	PROPN
eurjchem-1251	386	28	g.	g.	PROPN
eurjchem-1251	386	29	;	;	PUNCT
eurjchem-1251	386	30	strappahetti	strappahetti	NOUN
eurjchem-1251	386	31	,	,	PUNCT
eurjchem-1251	386	32	g.	g.	PROPN
eurjchem-1251	386	33	;	;	PUNCT
eurjchem-1251	386	34	corsano	corsano	PROPN
eurjchem-1251	386	35	,	,	PUNCT
eurjchem-1251	386	36	s.	s.	PROPN
eurjchem-1251	386	37	j.	j.	PROPN
eurjchem-1251	386	38	med	med	PROPN
eurjchem-1251	386	39	.	.	PROPN
eurjchem-1251	386	40	chem	chem	PROPN
eurjchem-1251	386	41	.	.	PUNCT
eurjchem-1251	387	1	2001	2001	NUM
eurjchem-1251	387	2	,	,	PUNCT
eurjchem-1251	387	3	44	44	NUM
eurjchem-1251	387	4	,	,	PUNCT
eurjchem-1251	387	5	2118‐3132	2118‐3132	NUM
eurjchem-1251	387	6	.	.	PUNCT
eurjchem-1251	388	1	[	[	X
eurjchem-1251	388	2	4	4	NUM
eurjchem-1251	388	3	]	]	PUNCT
eurjchem-1251	388	4	.	.	PUNCT
eurjchem-1251	388	5	cignarella	cignarella	PROPN
eurjchem-1251	388	6	,	,	PUNCT
eurjchem-1251	388	7	g.	g.	PROPN
eurjchem-1251	388	8	;	;	PUNCT
eurjchem-1251	388	9	barlocco	barlocco	PROPN
eurjchem-1251	388	10	,	,	PUNCT
eurjchem-1251	388	11	d.	d.	PROPN
eurjchem-1251	388	12	j.	j.	PROPN
eurjchem-1251	388	13	heterocycl	heterocycl	PROPN
eurjchem-1251	388	14	.	.	PUNCT
eurjchem-1251	389	1	chem	chem	PROPN
eurjchem-1251	389	2	.	.	PUNCT
eurjchem-1251	390	1	2002	2002	NUM
eurjchem-1251	390	2	,	,	PUNCT
eurjchem-1251	390	3	39	39	NUM
eurjchem-1251	390	4	,	,	PUNCT
eurjchem-1251	390	5	545‐550	545‐550	NUM
eurjchem-1251	390	6	.	.	PUNCT
eurjchem-1251	391	1	[	[	X
eurjchem-1251	391	2	5	5	NUM
eurjchem-1251	391	3	]	]	PUNCT
eurjchem-1251	391	4	.	.	PUNCT
eurjchem-1251	392	1	mann	mann	PROPN
eurjchem-1251	392	2	,	,	PUNCT
eurjchem-1251	392	3	e.	e.	PROPN
eurjchem-1251	392	4	;	;	PUNCT
eurjchem-1251	392	5	moisan	moisan	PROPN
eurjchem-1251	392	6	,	,	PUNCT
eurjchem-1251	392	7	l.	l.	PROPN
eurjchem-1251	392	8	;	;	PUNCT
eurjchem-1251	392	9	hou	hou	PROPN
eurjchem-1251	392	10	,	,	PUNCT
eurjchem-1251	392	11	j.	j.	PROPN
eurjchem-1251	392	12	;	;	PUNCT
eurjchem-1251	392	13	rebek	rebek	PROPN
eurjchem-1251	392	14	,	,	PUNCT
eurjchem-1251	392	15	j.	j.	PROPN
eurjchem-1251	392	16	tetrahedron	tetrahedron	PROPN
eurjchem-1251	392	17	lett	lett	PROPN
eurjchem-1251	392	18	.	.	PUNCT
eurjchem-1251	392	19	2008	2008	NUM
eurjchem-1251	392	20	,	,	PUNCT
eurjchem-1251	392	21	49	49	NUM
eurjchem-1251	392	22	,	,	PUNCT
eurjchem-1251	392	23	903‐905	903‐905	NUM
eurjchem-1251	392	24	.	.	PUNCT
eurjchem-1251	393	1	[	[	X
eurjchem-1251	393	2	6	6	NUM
eurjchem-1251	393	3	]	]	PUNCT
eurjchem-1251	393	4	.	.	PUNCT
eurjchem-1251	394	1	tucker	tucker	PROPN
eurjchem-1251	394	2	,	,	PUNCT
eurjchem-1251	394	3	j.	j.	PROPN
eurjchem-1251	394	4	a.	a.	PROPN
eurjchem-1251	394	5	;	;	PUNCT
eurjchem-1251	394	6	allwine	allwine	VERB
eurjchem-1251	394	7	,	,	PUNCT
eurjchem-1251	394	8	d.	d.	PROPN
eurjchem-1251	394	9	a.	a.	PROPN
eurjchem-1251	394	10	;	;	PUNCT
eurjchem-1251	394	11	grega	grega	PROPN
eurjchem-1251	394	12	,	,	PUNCT
eurjchem-1251	394	13	k.	k.	PROPN
eurjchem-1251	394	14	c.	c.	PROPN
eurjchem-1251	394	15	;	;	PUNCT
eurjchem-1251	394	16	barbachyn	barbachyn	PROPN
eurjchem-1251	394	17	,	,	PUNCT
eurjchem-1251	394	18	m.	m.	PROPN
eurjchem-1251	394	19	r.	r.	PROPN
eurjchem-1251	394	20	;	;	PUNCT
eurjchem-1251	394	21	klock	klock	PROPN
eurjchem-1251	394	22	,	,	PUNCT
eurjchem-1251	394	23	j.	j.	PROPN
eurjchem-1251	394	24	l.	l.	PROPN
eurjchem-1251	394	25	;	;	PUNCT
eurjchem-1251	394	26	adamski	adamski	PROPN
eurjchem-1251	394	27	,	,	PUNCT
eurjchem-1251	394	28	j.	j.	PROPN
eurjchem-1251	394	29	l.	l.	PROPN
eurjchem-1251	394	30	;	;	PUNCT
eurjchem-1251	394	31	brickner	brickner	PROPN
eurjchem-1251	394	32	,	,	PUNCT
eurjchem-1251	394	33	s.	s.	PROPN
eurjchem-1251	394	34	;	;	PUNCT
eurjchem-1251	394	35	hutchinson	hutchinson	PROPN
eurjchem-1251	394	36	,	,	PUNCT
eurjchem-1251	394	37	s.	s.	PROPN
eurjchem-1251	394	38	j.	j.	PROPN
eurjchem-1251	394	39	;	;	PUNCT
eurjchem-1251	394	40	ford	ford	PROPN
eurjchem-1251	394	41	,	,	PUNCT
eurjchem-1251	394	42	d.	d.	PROPN
eurjchem-1251	394	43	k.	k.	PROPN
eurjchem-1251	394	44	;	;	PUNCT
eurjchem-1251	394	45	zurenko	zurenko	PROPN
eurjchem-1251	394	46	,	,	PUNCT
eurjchem-1251	394	47	c.	c.	PROPN
eurjchem-1251	394	48	w.	w.	PROPN
eurjchem-1251	394	49	;	;	PUNCT
eurjchem-1251	394	50	conradi	conradi	NOUN
eurjchem-1251	394	51	,	,	PUNCT
eurjchem-1251	394	52	g.	g.	PROPN
eurjchem-1251	394	53	e.	e.	PROPN
eurjchem-1251	394	54	;	;	PUNCT
eurjchem-1251	394	55	burton	burton	PROPN
eurjchem-1251	394	56	,	,	PUNCT
eurjchem-1251	394	57	r.	r.	PROPN
eurjchem-1251	394	58	a.	a.	PROPN
eurjchem-1251	394	59	;	;	PUNCT
eurjchem-1251	394	60	jensen	jensen	PROPN
eurjchem-1251	394	61	,	,	PUNCT
eurjchem-1251	395	1	p.	p.	PROPN
eurjchem-1251	395	2	r.	r.	PROPN
eurjchem-1251	395	3	m.	m.	PROPN
eurjchem-1251	395	4	j.	j.	PROPN
eurjchem-1251	395	5	med	med	PROPN
eurjchem-1251	395	6	.	.	PROPN
eurjchem-1251	395	7	chem	chem	PROPN
eurjchem-1251	395	8	.	.	PUNCT
eurjchem-1251	396	1	1998	1998	NUM
eurjchem-1251	396	2	,	,	PUNCT
eurjchem-1251	396	3	41	41	NUM
eurjchem-1251	396	4	,	,	PUNCT
eurjchem-1251	396	5	3727‐3735	3727‐3735	NUM
eurjchem-1251	396	6	.	.	PUNCT
eurjchem-1251	397	1	[	[	X
eurjchem-1251	397	2	7	7	NUM
eurjchem-1251	397	3	]	]	PUNCT
eurjchem-1251	397	4	.	.	PUNCT
eurjchem-1251	398	1	tamayo	tamayo	PROPN
eurjchem-1251	398	2	,	,	PUNCT
eurjchem-1251	398	3	n.	n.	PROPN
eurjchem-1251	398	4	;	;	PUNCT
eurjchem-1251	398	5	liao	liao	PROPN
eurjchem-1251	398	6	,	,	PUNCT
eurjchem-1251	398	7	l.	l.	PROPN
eurjchem-1251	398	8	;	;	PUNCT
eurjchem-1251	398	9	goldberg	goldberg	PROPN
eurjchem-1251	398	10	,	,	PUNCT
eurjchem-1251	398	11	m.	m.	NOUN
eurjchem-1251	398	12	;	;	PUNCT
eurjchem-1251	398	13	powers	power	NOUN
eurjchem-1251	398	14	,	,	PUNCT
eurjchem-1251	398	15	d.	d.	PROPN
eurjchem-1251	398	16	;	;	PUNCT
eurjchem-1251	398	17	tudor	tudor	PROPN
eurjchem-1251	398	18	,	,	PUNCT
eurjchem-1251	398	19	y.	y.	PROPN
eurjchem-1251	398	20	y.	y.	PROPN
eurjchem-1251	398	21	;	;	PUNCT
eurjchem-1251	398	22	yu	yu	PROPN
eurjchem-1251	398	23	,	,	PUNCT
eurjchem-1251	398	24	v.	v.	PROPN
eurjchem-1251	398	25	;	;	PUNCT
eurjchem-1251	398	26	wong	wong	PROPN
eurjchem-1251	398	27	,	,	PUNCT
eurjchem-1251	398	28	l.	l.	PROPN
eurjchem-1251	398	29	m.	m.	PROPN
eurjchem-1251	398	30	;	;	PUNCT
eurjchem-1251	398	31	henkle	henkle	ADJ
eurjchem-1251	398	32	,	,	PUNCT
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eurjchem-1251	398	34	;	;	PUNCT
eurjchem-1251	398	35	middleton	middleton	PROPN
eurjchem-1251	398	36	,	,	PUNCT
eurjchem-1251	398	37	s.	s.	PROPN
eurjchem-1251	398	38	;	;	PUNCT
eurjchem-1251	398	39	syed	sye	VERB
eurjchem-1251	398	40	,	,	PUNCT
eurjchem-1251	398	41	r.	r.	PROPN
eurjchem-1251	398	42	;	;	PUNCT
eurjchem-1251	398	43	harvey	harvey	NOUN
eurjchem-1251	398	44	,	,	PUNCT
eurjchem-1251	398	45	t.	t.	PROPN
eurjchem-1251	398	46	;	;	PUNCT
eurjchem-1251	398	47	jang	jang	PROPN
eurjchem-1251	398	48	,	,	PUNCT
eurjchem-1251	398	49	g.	g.	PROPN
eurjchem-1251	398	50	;	;	PUNCT
eurjchem-1251	398	51	hungate	hungate	PROPN
eurjchem-1251	398	52	,	,	PUNCT
eurjchem-1251	398	53	r.	r.	PROPN
eurjchem-1251	398	54	;	;	PUNCT
eurjchem-1251	398	55	dominguez	dominguez	PROPN
eurjchem-1251	398	56	,	,	PUNCT
eurjchem-1251	398	57	c.	c.	PROPN
eurjchem-1251	398	58	bioorg	bioorg	PROPN
eurjchem-1251	398	59	.	.	PUNCT
eurjchem-1251	399	1	med	med	PROPN
eurjchem-1251	399	2	.	.	PROPN
eurjchem-1251	399	3	chem	chem	PROPN
eurjchem-1251	399	4	.	.	PUNCT
eurjchem-1251	400	1	lett	lett	PROPN
eurjchem-1251	400	2	.	.	PUNCT
eurjchem-1251	401	1	2005	2005	NUM
eurjchem-1251	401	2	,	,	PUNCT
eurjchem-1251	401	3	15	15	NUM
eurjchem-1251	401	4	,	,	PUNCT
eurjchem-1251	401	5	2409‐	2409‐	NUM
eurjchem-1251	401	6	2413	2413	NUM
eurjchem-1251	401	7	.	.	PUNCT
eurjchem-1251	402	1	[	[	X
eurjchem-1251	402	2	8	8	NUM
eurjchem-1251	402	3	]	]	PUNCT
eurjchem-1251	402	4	.	.	PUNCT
eurjchem-1251	403	1	benson	benson	PROPN
eurjchem-1251	403	2	,	,	PUNCT
eurjchem-1251	403	3	s.	s.	PROPN
eurjchem-1251	403	4	c.	c.	PROPN
eurjchem-1251	403	5	;	;	PUNCT
eurjchem-1251	403	6	palabrica	palabrica	NOUN
eurjchem-1251	403	7	,	,	PUNCT
eurjchem-1251	403	8	c.	c.	PROPN
eurjchem-1251	403	9	a.	a.	PROPN
eurjchem-1251	403	10	;	;	PUNCT
eurjchem-1251	403	11	snyder	snyder	PROPN
eurjchem-1251	403	12	,	,	PUNCT
eurjchem-1251	403	13	j.	j.	PROPN
eurjchem-1251	403	14	k.	k.	PROPN
eurjchem-1251	403	15	j.	j.	PROPN
eurjchem-1251	403	16	org	org	PROPN
eurjchem-1251	403	17	.	.	PUNCT
eurjchem-1251	403	18	chem	chem	PROPN
eurjchem-1251	403	19	.	.	PUNCT
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eurjchem-1251	404	2	,	,	PUNCT
eurjchem-1251	404	3	52	52	NUM
eurjchem-1251	404	4	,	,	PUNCT
eurjchem-1251	404	5	4610‐4614	4610‐4614	NUM
eurjchem-1251	404	6	.	.	PUNCT
eurjchem-1251	405	1	[	[	X
eurjchem-1251	405	2	9	9	NUM
eurjchem-1251	405	3	]	]	PUNCT
eurjchem-1251	405	4	.	.	PUNCT
eurjchem-1251	405	5	gyoten	gyoten	VERB
eurjchem-1251	405	6	,	,	PUNCT
eurjchem-1251	405	7	m.	m.	NOUN
eurjchem-1251	405	8	;	;	PUNCT
eurjchem-1251	405	9	nagaya	nagaya	PROPN
eurjchem-1251	405	10	,	,	PUNCT
eurjchem-1251	405	11	h.	h.	PROPN
eurjchem-1251	405	12	;	;	PUNCT
eurjchem-1251	405	13	fukuda	fukuda	PROPN
eurjchem-1251	405	14	,	,	PUNCT
eurjchem-1251	405	15	s.	s.	PROPN
eurjchem-1251	405	16	;	;	PUNCT
eurjchem-1251	405	17	ashida	ashida	PROPN
eurjchem-1251	405	18	,	,	PUNCT
eurjchem-1251	405	19	y.	y.	PROPN
eurjchem-1251	405	20	;	;	PUNCT
eurjchem-1251	405	21	kawano	kawano	PROPN
eurjchem-1251	405	22	,	,	PUNCT
eurjchem-1251	405	23	y.	y.	PROPN
eurjchem-1251	405	24	chem	chem	PROPN
eurjchem-1251	405	25	.	.	PUNCT
eurjchem-1251	406	1	pharm	pharm	NOUN
eurjchem-1251	406	2	.	.	PUNCT
eurjchem-1251	407	1	bull	bull	PROPN
eurjchem-1251	407	2	.	.	PUNCT
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eurjchem-1251	408	2	,	,	PUNCT
eurjchem-1251	408	3	51	51	NUM
eurjchem-1251	408	4	,	,	PUNCT
eurjchem-1251	408	5	122‐133	122‐133	NUM
eurjchem-1251	408	6	.	.	PUNCT
eurjchem-1251	409	1	[	[	X
eurjchem-1251	409	2	10	10	NUM
eurjchem-1251	409	3	]	]	PUNCT
eurjchem-1251	409	4	.	.	PUNCT
eurjchem-1251	410	1	piaz	piaz	PROPN
eurjchem-1251	410	2	,	,	PUNCT
eurjchem-1251	410	3	v.	v.	PROPN
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eurjchem-1251	410	5	;	;	PUNCT
eurjchem-1251	410	6	vergelli	vergelli	PROPN
eurjchem-1251	410	7	,	,	PUNCT
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eurjchem-1251	410	9	;	;	PUNCT
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eurjchem-1251	410	12	m.	m.	NOUN
eurjchem-1251	410	13	p.	p.	NOUN
eurjchem-1251	410	14	;	;	PUNCT
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eurjchem-1251	410	16	,	,	PUNCT
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eurjchem-1251	410	19	a.	a.	PROPN
eurjchem-1251	410	20	;	;	PUNCT
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eurjchem-1251	410	22	,	,	PUNCT
eurjchem-1251	410	23	g.	g.	PROPN
eurjchem-1251	410	24	;	;	PUNCT
eurjchem-1251	410	25	zaratin	zaratin	PROPN
eurjchem-1251	410	26	,	,	PUNCT
eurjchem-1251	410	27	p.	p.	PROPN
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eurjchem-1251	410	31	,	,	PUNCT
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eurjchem-1251	410	35	.	.	PUNCT
eurjchem-1251	411	1	[	[	X
eurjchem-1251	411	2	11	11	NUM
eurjchem-1251	411	3	]	]	PUNCT
eurjchem-1251	411	4	.	.	PUNCT
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eurjchem-1251	411	6	,	,	PUNCT
eurjchem-1251	411	7	a.	a.	PROPN
eurjchem-1251	411	8	;	;	PUNCT
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eurjchem-1251	411	10	,	,	PUNCT
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eurjchem-1251	411	12	;	;	PUNCT
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eurjchem-1251	411	14	,	,	PUNCT
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eurjchem-1251	411	16	;	;	PUNCT
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eurjchem-1251	411	18	,	,	PUNCT
eurjchem-1251	411	19	e.	e.	PROPN
eurjchem-1251	411	20	;	;	PUNCT
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eurjchem-1251	411	22	,	,	PUNCT
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eurjchem-1251	411	24	;	;	PUNCT
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eurjchem-1251	411	26	,	,	PUNCT
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eurjchem-1251	411	28	;	;	PUNCT
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eurjchem-1251	411	30	,	,	PUNCT
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eurjchem-1251	411	34	;	;	PUNCT
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eurjchem-1251	411	36	,	,	PUNCT
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eurjchem-1251	411	38	;	;	PUNCT
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eurjchem-1251	411	40	,	,	PUNCT
eurjchem-1251	411	41	e.	e.	PROPN
eurjchem-1251	411	42	;	;	PUNCT
eurjchem-1251	411	43	lemière	lemière	PROPN
eurjchem-1251	411	44	,	,	PUNCT
eurjchem-1251	411	45	g.	g.	PROPN
eurjchem-1251	411	46	l.	l.	PROPN
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eurjchem-1251	411	48	;	;	PUNCT
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eurjchem-1251	411	50	,	,	PUNCT
eurjchem-1251	411	51	e.	e.	PROPN
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eurjchem-1251	411	53	.	.	PUNCT
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eurjchem-1251	412	4	.	.	PUNCT
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eurjchem-1251	413	2	.	.	PUNCT
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eurjchem-1251	414	2	,	,	PUNCT
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eurjchem-1251	414	4	,	,	PUNCT
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eurjchem-1251	414	6	.	.	PUNCT
eurjchem-1251	415	1	[	[	X
eurjchem-1251	415	2	12	12	NUM
eurjchem-1251	415	3	]	]	PUNCT
eurjchem-1251	415	4	.	.	PUNCT
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eurjchem-1251	415	6	,	,	PUNCT
eurjchem-1251	415	7	g.	g.	PROPN
eurjchem-1251	415	8	;	;	PUNCT
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eurjchem-1251	415	10	,	,	PUNCT
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eurjchem-1251	415	12	;	;	PUNCT
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eurjchem-1251	415	14	,	,	PUNCT
eurjchem-1251	415	15	c.	c.	PROPN
eurjchem-1251	415	16	;	;	PUNCT
eurjchem-1251	415	17	basu	basu	PROPN
eurjchem-1251	415	18	,	,	PUNCT
eurjchem-1251	415	19	c.	c.	PROPN
eurjchem-1251	415	20	;	;	PUNCT
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eurjchem-1251	415	22	,	,	PUNCT
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eurjchem-1251	415	25	.	.	PUNCT
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eurjchem-1251	416	2	.	.	PUNCT
eurjchem-1251	417	1	lett	lett	PROPN
eurjchem-1251	417	2	.	.	PUNCT
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eurjchem-1251	418	2	,	,	PUNCT
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eurjchem-1251	418	4	,	,	PUNCT
eurjchem-1251	418	5	155‐165	155‐165	NUM
eurjchem-1251	418	6	.	.	PUNCT
eurjchem-1251	419	1	[	[	X
eurjchem-1251	419	2	13	13	NUM
eurjchem-1251	419	3	]	]	PUNCT
eurjchem-1251	419	4	.	.	PUNCT
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eurjchem-1251	419	9	;	;	PUNCT
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eurjchem-1251	419	14	;	;	PUNCT
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eurjchem-1251	419	18	;	;	PUNCT
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eurjchem-1251	419	23	.	.	PUNCT
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eurjchem-1251	420	2	.	.	PUNCT
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eurjchem-1251	421	2	.	.	PROPN
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eurjchem-1251	421	4	,	,	PUNCT
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eurjchem-1251	421	6	,	,	PUNCT
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eurjchem-1251	421	8	.	.	PUNCT
eurjchem-1251	422	1	[	[	X
eurjchem-1251	422	2	14	14	NUM
eurjchem-1251	422	3	]	]	PUNCT
eurjchem-1251	422	4	.	.	PUNCT
eurjchem-1251	423	1	schmidt	schmidt	PROPN
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eurjchem-1251	423	4	;	;	PUNCT
eurjchem-1251	423	5	druey	druey	PROPN
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eurjchem-1251	423	9	.	.	PUNCT
eurjchem-1251	424	1	chim	chim	PROPN
eurjchem-1251	424	2	.	.	PUNCT
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eurjchem-1251	425	3	,	,	PUNCT
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eurjchem-1251	425	5	,	,	PUNCT
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eurjchem-1251	425	7	.	.	PUNCT
eurjchem-1251	426	1	[	[	X
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eurjchem-1251	426	4	.	.	PUNCT
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eurjchem-1251	427	2	,	,	PUNCT
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eurjchem-1251	427	4	;	;	PUNCT
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eurjchem-1251	427	6	,	,	PUNCT
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eurjchem-1251	427	8	;	;	PUNCT
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eurjchem-1251	427	13	.	.	PUNCT
eurjchem-1251	428	1	ann	ann	PROPN
eurjchem-1251	428	2	.	.	PUNCT
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eurjchem-1251	428	4	.	.	PUNCT
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eurjchem-1251	429	2	,	,	PUNCT
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eurjchem-1251	429	7	.	.	PUNCT
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eurjchem-1251	430	2	16	16	NUM
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eurjchem-1251	430	8	;	;	PUNCT
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eurjchem-1251	430	13	.	.	PUNCT
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eurjchem-1251	431	2	.	.	PUNCT
eurjchem-1251	432	1	acta	acta	PROPN
eurjchem-1251	432	2	.	.	PUNCT
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eurjchem-1251	434	4	.	.	PUNCT
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