id	sid	tid	token	lemma	pos
eurjchem-1252	1	1	untitled	untitle	VERB
eurjchem-1252	1	2	european	european	PROPN
eurjchem-1252	1	3	journal	journal	PROPN
eurjchem-1252	1	4	of	of	ADP
eurjchem-1252	1	5	chemistry	chemistry	NOUN
eurjchem-1252	1	6	6	6	NUM
eurjchem-1252	1	7	(	(	PUNCT
eurjchem-1252	1	8	2	2	NUM
eurjchem-1252	1	9	)	)	PUNCT
eurjchem-1252	1	10	(	(	PUNCT
eurjchem-1252	1	11	2015	2015	NUM
eurjchem-1252	1	12	)	)	PUNCT
eurjchem-1252	1	13	204‐210	204‐210	PROPN
eurjchem-1252	1	14	european	european	PROPN
eurjchem-1252	1	15	journal	journal	PROPN
eurjchem-1252	1	16	of	of	ADP
eurjchem-1252	1	17	chemistry	chemistry	NOUN
eurjchem-1252	1	18	issn	issn	PROPN
eurjchem-1252	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-1252	1	20	(	(	PUNCT
eurjchem-1252	1	21	print	print	NOUN
eurjchem-1252	1	22	)	)	PUNCT
eurjchem-1252	1	23	/	/	SYM
eurjchem-1252	1	24	issn	issn	PROPN
eurjchem-1252	1	25	2153‐2257	2153‐2257	NUM
eurjchem-1252	1	26	(	(	PUNCT
eurjchem-1252	1	27	online	online	ADJ
eurjchem-1252	1	28	)	)	PUNCT
eurjchem-1252	1	29			NOUN
eurjchem-1252	1	30	2015	2015	NUM
eurjchem-1252	1	31	atlanta	atlanta	PROPN
eurjchem-1252	1	32	publishing	publishing	PROPN
eurjchem-1252	1	33	house	house	PROPN
eurjchem-1252	1	34	llc	llc	PROPN
eurjchem-1252	1	35	‐	‐	PUNCT
eurjchem-1252	1	36	all	all	DET
eurjchem-1252	1	37	rights	right	NOUN
eurjchem-1252	1	38	reserved	reserve	VERB
eurjchem-1252	1	39	‐	‐	NOUN
eurjchem-1252	1	40	printed	print	VERB
eurjchem-1252	1	41	in	in	ADP
eurjchem-1252	1	42	the	the	DET
eurjchem-1252	1	43	usa	usa	PROPN
eurjchem-1252	1	44	http://dx.doi.org/10.5155/eurjchem.6.2.204‐210.1252	http://dx.doi.org/10.5155/eurjchem.6.2.204‐210.1252	PROPN
eurjchem-1252	1	45	european	european	PROPN
eurjchem-1252	1	46	journal	journal	PROPN
eurjchem-1252	1	47	of	of	ADP
eurjchem-1252	1	48	chemistry	chemistry	PROPN
eurjchem-1252	1	49	journal	journal	PROPN
eurjchem-1252	1	50	webpage	webpage	NOUN
eurjchem-1252	1	51	:	:	PUNCT
eurjchem-1252	1	52	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1252	1	53	pyridazine	pyridazine	PROPN
eurjchem-1252	1	54	and	and	CCONJ
eurjchem-1252	1	55	its	its	PRON
eurjchem-1252	1	56	related	related	ADJ
eurjchem-1252	1	57	compounds	compound	NOUN
eurjchem-1252	1	58	:	:	PUNCT
eurjchem-1252	1	59	part	part	NOUN
eurjchem-1252	1	60	38	38	NUM
eurjchem-1252	1	61	.	.	PUNCT
eurjchem-1252	2	1	pyrimido[1,2‐b]pyridazinone	pyrimido[1,2‐b]pyridazinone	NOUN
eurjchem-1252	2	2	,	,	PUNCT
eurjchem-1252	2	3	synthesis	synthesis	NOUN
eurjchem-1252	2	4	and	and	CCONJ
eurjchem-1252	2	5	some	some	DET
eurjchem-1252	2	6	reactions	reaction	NOUN
eurjchem-1252	2	7	ali	ali	PROPN
eurjchem-1252	2	8	abdel	abdel	PROPN
eurjchem-1252	2	9	hamid	hamid	PROPN
eurjchem-1252	2	10	deeb	deeb	PROPN
eurjchem-1252	2	11	1	1	NUM
eurjchem-1252	2	12	,	,	PUNCT
eurjchem-1252	2	13	*	*	PUNCT
eurjchem-1252	2	14	,	,	PUNCT
eurjchem-1252	2	15	fatma	fatma	PROPN
eurjchem-1252	2	16	abdel	abdel	PROPN
eurjchem-1252	2	17	rahman	rahman	PROPN
eurjchem-1252	2	18	el‐mariah	el‐mariah	PROPN
eurjchem-1252	2	19	2	2	NUM
eurjchem-1252	2	20	and	and	CCONJ
eurjchem-1252	2	21	heba	heba	PROPN
eurjchem-1252	2	22	kamal	kamal	PROPN
eurjchem-1252	2	23	abd	abd	PROPN
eurjchem-1252	3	1	el‐mawgoud	el‐mawgoud	ADJ
eurjchem-1252	3	2	2	2	NUM
eurjchem-1252	3	3	1	1	NUM
eurjchem-1252	3	4	department	department	NOUN
eurjchem-1252	3	5	of	of	ADP
eurjchem-1252	3	6	chemistry	chemistry	NOUN
eurjchem-1252	3	7	,	,	PUNCT
eurjchem-1252	3	8	faculty	faculty	NOUN
eurjchem-1252	3	9	of	of	ADP
eurjchem-1252	3	10	science	science	NOUN
eurjchem-1252	3	11	,	,	PUNCT
eurjchem-1252	3	12	zagazig	zagazig	PROPN
eurjchem-1252	3	13	university	university	PROPN
eurjchem-1252	3	14	,	,	PUNCT
eurjchem-1252	3	15	zagazig	zagazig	PROPN
eurjchem-1252	3	16	,	,	PUNCT
eurjchem-1252	3	17	44519	44519	NUM
eurjchem-1252	3	18	,	,	PUNCT
eurjchem-1252	3	19	egypt	egypt	PROPN
eurjchem-1252	3	20	2	2	NUM
eurjchem-1252	3	21	department	department	NOUN
eurjchem-1252	3	22	of	of	ADP
eurjchem-1252	3	23	chemistry	chemistry	NOUN
eurjchem-1252	3	24	,	,	PUNCT
eurjchem-1252	3	25	college	college	NOUN
eurjchem-1252	3	26	of	of	ADP
eurjchem-1252	3	27	women	woman	NOUN
eurjchem-1252	3	28	for	for	ADP
eurjchem-1252	3	29	arts	art	NOUN
eurjchem-1252	3	30	,	,	PUNCT
eurjchem-1252	3	31	science	science	NOUN
eurjchem-1252	3	32	,	,	PUNCT
eurjchem-1252	3	33	and	and	CCONJ
eurjchem-1252	3	34	education	education	NOUN
eurjchem-1252	3	35	,	,	PUNCT
eurjchem-1252	3	36	ain	ain	PROPN
eurjchem-1252	3	37	shams	shams	PROPN
eurjchem-1252	3	38	university	university	PROPN
eurjchem-1252	3	39	,	,	PUNCT
eurjchem-1252	3	40	cairo	cairo	PROPN
eurjchem-1252	3	41	,	,	PUNCT
eurjchem-1252	3	42	11753	11753	NUM
eurjchem-1252	3	43	,	,	PUNCT
eurjchem-1252	3	44	egypt	egypt	PROPN
eurjchem-1252	3	45	*	*	PUNCT
eurjchem-1252	3	46	corresponding	correspond	VERB
eurjchem-1252	3	47	author	author	NOUN
eurjchem-1252	3	48	at	at	ADP
eurjchem-1252	3	49	:	:	PUNCT
eurjchem-1252	3	50	department	department	NOUN
eurjchem-1252	3	51	of	of	ADP
eurjchem-1252	3	52	chemistry	chemistry	NOUN
eurjchem-1252	3	53	,	,	PUNCT
eurjchem-1252	3	54	faculty	faculty	NOUN
eurjchem-1252	3	55	of	of	ADP
eurjchem-1252	3	56	science	science	NOUN
eurjchem-1252	3	57	,	,	PUNCT
eurjchem-1252	3	58	zagazig	zagazig	PROPN
eurjchem-1252	3	59	university	university	PROPN
eurjchem-1252	3	60	,	,	PUNCT
eurjchem-1252	3	61	zagazig	zagazig	PROPN
eurjchem-1252	3	62	,	,	PUNCT
eurjchem-1252	3	63	44519	44519	NUM
eurjchem-1252	3	64	,	,	PUNCT
eurjchem-1252	3	65	egypt	egypt	PROPN
eurjchem-1252	3	66	.	.	PUNCT
eurjchem-1252	4	1	tel	tel	PROPN
eurjchem-1252	4	2	.	.	PUNCT
eurjchem-1252	4	3	:	:	PUNCT
eurjchem-1252	5	1	+20.55.2303252	+20.55.2303252	NUM
eurjchem-1252	5	2	.	.	PUNCT
eurjchem-1252	5	3	fax	fax	NOUN
eurjchem-1252	5	4	:	:	PUNCT
eurjchem-1252	5	5	+20.55.2308213	+20.55.2308213	NUM
eurjchem-1252	5	6	.	.	PUNCT
eurjchem-1252	5	7	e‐mail	e‐mail	PUNCT
eurjchem-1252	5	8	address	address	NOUN
eurjchem-1252	5	9	:	:	PUNCT
eurjchem-1252	5	10	dralideeb@hotmail.com	dralideeb@hotmail.com	PROPN
eurjchem-1252	5	11	(	(	PUNCT
eurjchem-1252	5	12	a.a	a.a	PROPN
eurjchem-1252	5	13	.	.	PROPN
eurjchem-1252	5	14	deeb	deeb	PROPN
eurjchem-1252	5	15	)	)	PUNCT
eurjchem-1252	5	16	.	.	PUNCT
eurjchem-1252	6	1	article	article	NOUN
eurjchem-1252	6	2	information	information	PROPN
eurjchem-1252	6	3	abstract	abstract	ADJ
eurjchem-1252	6	4	doi	doi	NOUN
eurjchem-1252	6	5	:	:	PUNCT
eurjchem-1252	6	6	10.5155	10.5155	NUM
eurjchem-1252	6	7	/	/	SYM
eurjchem-1252	6	8	eurjchem.6.2.204‐210.1252	eurjchem.6.2.204‐210.1252	AUX
eurjchem-1252	6	9	received	receive	VERB
eurjchem-1252	6	10	:	:	PUNCT
eurjchem-1252	6	11	04	04	NUM
eurjchem-1252	6	12	february	february	NOUN
eurjchem-1252	6	13	2015	2015	NUM
eurjchem-1252	6	14	received	receive	VERB
eurjchem-1252	6	15	in	in	ADP
eurjchem-1252	6	16	revised	revise	VERB
eurjchem-1252	6	17	form	form	NOUN
eurjchem-1252	6	18	:	:	PUNCT
eurjchem-1252	6	19	20	20	NUM
eurjchem-1252	6	20	april	april	PROPN
eurjchem-1252	6	21	2015	2015	NUM
eurjchem-1252	6	22	accepted	accept	VERB
eurjchem-1252	6	23	:	:	PUNCT
eurjchem-1252	6	24	25	25	NUM
eurjchem-1252	6	25	april	april	PROPN
eurjchem-1252	6	26	2015	2015	NUM
eurjchem-1252	6	27	published	publish	VERB
eurjchem-1252	6	28	online	online	ADV
eurjchem-1252	6	29	:	:	PUNCT
eurjchem-1252	6	30	30	30	NUM
eurjchem-1252	6	31	june	june	PROPN
eurjchem-1252	6	32	2015	2015	NUM
eurjchem-1252	6	33	printed	print	VERB
eurjchem-1252	6	34	:	:	PUNCT
eurjchem-1252	6	35	30	30	NUM
eurjchem-1252	6	36	june	june	PROPN
eurjchem-1252	6	37	2015	2015	NUM
eurjchem-1252	6	38	a	a	DET
eurjchem-1252	6	39	new	new	ADJ
eurjchem-1252	6	40	method	method	NOUN
eurjchem-1252	6	41	of	of	ADP
eurjchem-1252	6	42	generating	generate	VERB
eurjchem-1252	6	43	the	the	DET
eurjchem-1252	6	44	fused	fuse	VERB
eurjchem-1252	6	45	heterocyclic	heterocyclic	ADJ
eurjchem-1252	6	46	system	system	NOUN
eurjchem-1252	6	47	with	with	ADP
eurjchem-1252	6	48	bridge	bridge	NOUN
eurjchem-1252	6	49	head	head	NOUN
eurjchem-1252	6	50	nitrogen	nitrogen	NOUN
eurjchem-1252	6	51	pyrimido[1,2‐b]pyridazinone	pyrimido[1,2‐b]pyridazinone	NOUN
eurjchem-1252	6	52	,	,	PUNCT
eurjchem-1252	6	53	from	from	ADP
eurjchem-1252	6	54	3‐amino‐4,5,6‐triphenylpyridazine	3‐amino‐4,5,6‐triphenylpyridazine	NUM
eurjchem-1252	6	55	and	and	CCONJ
eurjchem-1252	6	56	malonic	malonic	ADJ
eurjchem-1252	6	57	acid	acid	NOUN
eurjchem-1252	6	58	in	in	ADP
eurjchem-1252	6	59	presence	presence	NOUN
eurjchem-1252	6	60	of	of	ADP
eurjchem-1252	6	61	phosphoryl	phosphoryl	PROPN
eurjchem-1252	6	62	chloride	chloride	PROPN
eurjchem-1252	6	63	is	be	AUX
eurjchem-1252	6	64	described	describe	VERB
eurjchem-1252	6	65	.	.	PUNCT
eurjchem-1252	7	1	the	the	DET
eurjchem-1252	7	2	structures	structure	NOUN
eurjchem-1252	7	3	of	of	ADP
eurjchem-1252	7	4	the	the	DET
eurjchem-1252	7	5	synthesized	synthesize	VERB
eurjchem-1252	7	6	compounds	compound	NOUN
eurjchem-1252	7	7	were	be	AUX
eurjchem-1252	7	8	confirmed	confirm	VERB
eurjchem-1252	7	9	by	by	ADP
eurjchem-1252	7	10	their	their	PRON
eurjchem-1252	7	11	infrared	infrared	NOUN
eurjchem-1252	7	12	,	,	PUNCT
eurjchem-1252	7	13	mass	mass	NOUN
eurjchem-1252	7	14	spectrum	spectrum	NOUN
eurjchem-1252	7	15	,	,	PUNCT
eurjchem-1252	7	16	1h	1h	NUM
eurjchem-1252	7	17	nmr	nmr	NOUN
eurjchem-1252	7	18	and	and	CCONJ
eurjchem-1252	7	19	elemental	elemental	ADJ
eurjchem-1252	7	20	analyses	analysis	NOUN
eurjchem-1252	7	21	.	.	PUNCT
eurjchem-1252	8	1	the	the	DET
eurjchem-1252	8	2	antimicrobial	antimicrobial	ADJ
eurjchem-1252	8	3	activity	activity	NOUN
eurjchem-1252	8	4	of	of	ADP
eurjchem-1252	8	5	the	the	DET
eurjchem-1252	8	6	compounds	compound	NOUN
eurjchem-1252	8	7	obtained	obtain	VERB
eurjchem-1252	8	8	was	be	AUX
eurjchem-1252	8	9	examined	examine	VERB
eurjchem-1252	8	10	against	against	ADP
eurjchem-1252	8	11	some	some	DET
eurjchem-1252	8	12	selected	select	VERB
eurjchem-1252	8	13	microorganisms	microorganism	NOUN
eurjchem-1252	8	14	.	.	PUNCT
eurjchem-1252	9	1	keywords	keyword	VERB
eurjchem-1252	9	2	3‐aminopyridazine	3‐aminopyridazine	NUM
eurjchem-1252	9	3	anti‐microbial	anti‐microbial	ADJ
eurjchem-1252	9	4	activity	activity	NOUN
eurjchem-1252	9	5	electrophilic	electrophilic	ADJ
eurjchem-1252	9	6	substitutions	substitution	NOUN
eurjchem-1252	9	7	nuecleophilic	nuecleophilic	ADJ
eurjchem-1252	9	8	substitutions	substitution	NOUN
eurjchem-1252	9	9	pyaranopyrimidopyridazine	pyaranopyrimidopyridazine	ADJ
eurjchem-1252	9	10	pyrimido[1,2‐b]pyridazinone	pyrimido[1,2‐b]pyridazinone	NOUN
eurjchem-1252	9	11	cite	cite	VERB
eurjchem-1252	9	12	this	this	PRON
eurjchem-1252	9	13	:	:	PUNCT
eurjchem-1252	9	14	eur	eur	PROPN
eurjchem-1252	9	15	.	.	PUNCT
eurjchem-1252	10	1	j.	j.	PROPN
eurjchem-1252	10	2	chem	chem	PROPN
eurjchem-1252	10	3	.	.	PUNCT
eurjchem-1252	11	1	2015	2015	NUM
eurjchem-1252	11	2	,	,	PUNCT
eurjchem-1252	11	3	6(2	6(2	NUM
eurjchem-1252	11	4	)	)	PUNCT
eurjchem-1252	11	5	,	,	PUNCT
eurjchem-1252	11	6	204‐210	204‐210	PROPN
eurjchem-1252	11	7	1	1	NUM
eurjchem-1252	11	8	.	.	PUNCT
eurjchem-1252	12	1	introduction	introduction	NOUN
eurjchem-1252	12	2	the	the	DET
eurjchem-1252	12	3	pyridazines	pyridazine	NOUN
eurjchem-1252	12	4	and	and	CCONJ
eurjchem-1252	12	5	pyrimidines	pyrimidine	NOUN
eurjchem-1252	12	6	are	be	AUX
eurjchem-1252	12	7	important	important	ADJ
eurjchem-1252	12	8	and	and	CCONJ
eurjchem-1252	12	9	significant	significant	ADJ
eurjchem-1252	12	10	classes	class	NOUN
eurjchem-1252	12	11	of	of	ADP
eurjchem-1252	12	12	heterocyclic	heterocyclic	ADJ
eurjchem-1252	12	13	compounds	compound	NOUN
eurjchem-1252	12	14	[	[	X
eurjchem-1252	12	15	1‐3	1‐3	NOUN
eurjchem-1252	12	16	]	]	X
eurjchem-1252	12	17	.	.	PUNCT
eurjchem-1252	13	1	a	a	DET
eurjchem-1252	13	2	number	number	NOUN
eurjchem-1252	13	3	of	of	ADP
eurjchem-1252	13	4	their	their	PRON
eurjchem-1252	13	5	derivatives	derivative	NOUN
eurjchem-1252	13	6	have	have	AUX
eurjchem-1252	13	7	found	find	VERB
eurjchem-1252	13	8	diverse	diverse	ADJ
eurjchem-1252	13	9	uses	use	NOUN
eurjchem-1252	13	10	in	in	ADP
eurjchem-1252	13	11	synthetic	synthetic	ADJ
eurjchem-1252	13	12	,	,	PUNCT
eurjchem-1252	13	13	analytical	analytical	ADJ
eurjchem-1252	13	14	,	,	PUNCT
eurjchem-1252	13	15	medicinal	medicinal	ADJ
eurjchem-1252	13	16	,	,	PUNCT
eurjchem-1252	13	17	pharmaceutical	pharmaceutical	NOUN
eurjchem-1252	13	18	,	,	PUNCT
eurjchem-1252	13	19	agrochemical	agrochemical	NOUN
eurjchem-1252	13	20	,	,	PUNCT
eurjchem-1252	13	21	and	and	CCONJ
eurjchem-1252	13	22	photographic	photographic	ADJ
eurjchem-1252	13	23	chemistry	chemistry	NOUN
eurjchem-1252	13	24	.	.	PUNCT
eurjchem-1252	14	1	sometimes	sometimes	ADV
eurjchem-1252	14	2	the	the	DET
eurjchem-1252	14	3	fusion	fusion	NOUN
eurjchem-1252	14	4	of	of	ADP
eurjchem-1252	14	5	heterocyclic	heterocyclic	ADJ
eurjchem-1252	14	6	nuclei	nucleus	NOUN
eurjchem-1252	14	7	enhances	enhance	VERB
eurjchem-1252	14	8	the	the	DET
eurjchem-1252	14	9	pharmacological	pharmacological	ADJ
eurjchem-1252	14	10	activities	activity	NOUN
eurjchem-1252	14	11	much	much	ADV
eurjchem-1252	14	12	more	more	ADJ
eurjchem-1252	14	13	than	than	ADP
eurjchem-1252	14	14	its	its	PRON
eurjchem-1252	14	15	parent	parent	NOUN
eurjchem-1252	14	16	nucleus	nucleus	NOUN
eurjchem-1252	14	17	.	.	PUNCT
eurjchem-1252	15	1	hence	hence	ADV
eurjchem-1252	15	2	,	,	PUNCT
eurjchem-1252	15	3	it	it	PRON
eurjchem-1252	15	4	was	be	AUX
eurjchem-1252	15	5	thought	think	VERB
eurjchem-1252	15	6	that	that	SCONJ
eurjchem-1252	15	7	the	the	DET
eurjchem-1252	15	8	incorporation	incorporation	NOUN
eurjchem-1252	15	9	of	of	ADP
eurjchem-1252	15	10	the	the	DET
eurjchem-1252	15	11	latter	latter	ADJ
eurjchem-1252	15	12	heterocyclic	heterocyclic	ADJ
eurjchem-1252	15	13	moieties	moiety	NOUN
eurjchem-1252	15	14	into	into	ADP
eurjchem-1252	15	15	a	a	DET
eurjchem-1252	15	16	pyridazine	pyridazine	NOUN
eurjchem-1252	15	17	system	system	NOUN
eurjchem-1252	15	18	might	might	AUX
eurjchem-1252	15	19	modify	modify	VERB
eurjchem-1252	15	20	their	their	PRON
eurjchem-1252	15	21	biological	biological	ADJ
eurjchem-1252	15	22	activities	activity	NOUN
eurjchem-1252	15	23	.	.	PUNCT
eurjchem-1252	16	1	the	the	DET
eurjchem-1252	16	2	present	present	ADJ
eurjchem-1252	16	3	investigation	investigation	NOUN
eurjchem-1252	16	4	is	be	AUX
eurjchem-1252	16	5	in	in	ADP
eurjchem-1252	16	6	continuation	continuation	NOUN
eurjchem-1252	16	7	of	of	ADP
eurjchem-1252	16	8	our	our	PRON
eurjchem-1252	16	9	previous	previous	ADJ
eurjchem-1252	16	10	work	work	NOUN
eurjchem-1252	16	11	[	[	X
eurjchem-1252	16	12	4‐6	4‐6	X
eurjchem-1252	16	13	]	]	X
eurjchem-1252	16	14	on	on	ADP
eurjchem-1252	16	15	the	the	DET
eurjchem-1252	16	16	synthesis	synthesis	NOUN
eurjchem-1252	16	17	and	and	CCONJ
eurjchem-1252	16	18	biological	biological	ADJ
eurjchem-1252	16	19	activity	activity	NOUN
eurjchem-1252	16	20	of	of	ADP
eurjchem-1252	16	21	other	other	ADJ
eurjchem-1252	16	22	pyridazine	pyridazine	NOUN
eurjchem-1252	16	23	derivatives	derivative	NOUN
eurjchem-1252	16	24	.	.	PUNCT
eurjchem-1252	17	1	in	in	ADP
eurjchem-1252	17	2	the	the	DET
eurjchem-1252	17	3	accompanying	accompany	VERB
eurjchem-1252	17	4	paper	paper	NOUN
eurjchem-1252	17	5	[	[	X
eurjchem-1252	17	6	5	5	NUM
eurjchem-1252	17	7	]	]	PUNCT
eurjchem-1252	17	8	,	,	PUNCT
eurjchem-1252	17	9	we	we	PRON
eurjchem-1252	17	10	have	have	AUX
eurjchem-1252	17	11	described	describe	VERB
eurjchem-1252	17	12	the	the	DET
eurjchem-1252	17	13	preparation	preparation	NOUN
eurjchem-1252	17	14	of	of	ADP
eurjchem-1252	17	15	3‐amino‐4,5,6‐triphenyl	3‐amino‐4,5,6‐triphenyl	NUM
eurjchem-1252	17	16	pyridazine	pyridazine	NOUN
eurjchem-1252	17	17	a	a	DET
eurjchem-1252	17	18	useful	useful	ADJ
eurjchem-1252	17	19	starting	starting	NOUN
eurjchem-1252	17	20	material	material	NOUN
eurjchem-1252	17	21	for	for	ADP
eurjchem-1252	17	22	the	the	DET
eurjchem-1252	17	23	preparation	preparation	NOUN
eurjchem-1252	17	24	of	of	ADP
eurjchem-1252	17	25	7,8,9‐triphenyl‐2h‐pyrimido[1,2‐b]pyridazine‐2,4(3h)‐dione	7,8,9‐triphenyl‐2h‐pyrimido[1,2‐b]pyridazine‐2,4(3h)‐dione	NUM
eurjchem-1252	17	26	,	,	PUNCT
eurjchem-1252	17	27	1	1	NUM
eurjchem-1252	17	28	.	.	PUNCT
eurjchem-1252	18	1	in	in	ADP
eurjchem-1252	18	2	this	this	DET
eurjchem-1252	18	3	paper	paper	NOUN
eurjchem-1252	18	4	,	,	PUNCT
eurjchem-1252	18	5	we	we	PRON
eurjchem-1252	18	6	wish	wish	VERB
eurjchem-1252	18	7	to	to	PART
eurjchem-1252	18	8	show	show	VERB
eurjchem-1252	18	9	that	that	SCONJ
eurjchem-1252	18	10	compound	compound	NOUN
eurjchem-1252	18	11	1	1	NUM
eurjchem-1252	18	12	is	be	AUX
eurjchem-1252	18	13	also	also	ADV
eurjchem-1252	18	14	useful	useful	ADJ
eurjchem-1252	18	15	building	building	NOUN
eurjchem-1252	18	16	blocks	block	NOUN
eurjchem-1252	18	17	for	for	ADP
eurjchem-1252	18	18	the	the	DET
eurjchem-1252	18	19	synthesis	synthesis	NOUN
eurjchem-1252	18	20	of	of	ADP
eurjchem-1252	18	21	a	a	DET
eurjchem-1252	18	22	wide	wide	ADJ
eurjchem-1252	18	23	variety	variety	NOUN
eurjchem-1252	18	24	of	of	ADP
eurjchem-1252	18	25	pyrimidopyridazine	pyrimidopyridazine	NOUN
eurjchem-1252	18	26	derivatives	derivative	NOUN
eurjchem-1252	18	27	and	and	CCONJ
eurjchem-1252	18	28	to	to	PART
eurjchem-1252	18	29	test	test	VERB
eurjchem-1252	18	30	their	their	PRON
eurjchem-1252	18	31	anti‐microbial	anti‐microbial	ADJ
eurjchem-1252	18	32	activity	activity	NOUN
eurjchem-1252	18	33	.	.	PUNCT
eurjchem-1252	19	1	2	2	X
eurjchem-1252	19	2	.	.	X
eurjchem-1252	19	3	experimental	experimental	ADJ
eurjchem-1252	19	4	2.1	2.1	NUM
eurjchem-1252	19	5	.	.	PUNCT
eurjchem-1252	20	1	instrumentation	instrumentation	NOUN
eurjchem-1252	20	2	melting	melting	NOUN
eurjchem-1252	20	3	points	point	NOUN
eurjchem-1252	20	4	were	be	AUX
eurjchem-1252	20	5	determined	determine	VERB
eurjchem-1252	20	6	in	in	ADP
eurjchem-1252	20	7	open	open	ADJ
eurjchem-1252	20	8	glass	glass	NOUN
eurjchem-1252	20	9	capillaries	capillary	NOUN
eurjchem-1252	20	10	and	and	CCONJ
eurjchem-1252	20	11	are	be	AUX
eurjchem-1252	20	12	uncorrected	uncorrecte	VERB
eurjchem-1252	20	13	.	.	PUNCT
eurjchem-1252	21	1	elemental	elemental	ADJ
eurjchem-1252	21	2	analyses	analysis	NOUN
eurjchem-1252	21	3	were	be	AUX
eurjchem-1252	21	4	carried	carry	VERB
eurjchem-1252	21	5	out	out	ADP
eurjchem-1252	21	6	in	in	ADP
eurjchem-1252	21	7	the	the	DET
eurjchem-1252	21	8	micro	micro	ADJ
eurjchem-1252	21	9	analytical	analytical	ADJ
eurjchem-1252	21	10	laboratory	laboratory	NOUN
eurjchem-1252	21	11	of	of	ADP
eurjchem-1252	21	12	the	the	DET
eurjchem-1252	21	13	faculty	faculty	NOUN
eurjchem-1252	21	14	of	of	ADP
eurjchem-1252	21	15	science	science	NOUN
eurjchem-1252	21	16	,	,	PUNCT
eurjchem-1252	21	17	cairo	cairo	PROPN
eurjchem-1252	21	18	university	university	PROPN
eurjchem-1252	21	19	,	,	PUNCT
eurjchem-1252	21	20	egypt	egypt	PROPN
eurjchem-1252	21	21	.	.	PUNCT
eurjchem-1252	22	1	the	the	DET
eurjchem-1252	22	2	ir	ir	PROPN
eurjchem-1252	22	3	spectra	spectra	NOUN
eurjchem-1252	22	4	of	of	ADP
eurjchem-1252	22	5	compounds	compound	NOUN
eurjchem-1252	22	6	were	be	AUX
eurjchem-1252	22	7	recorded	record	VERB
eurjchem-1252	22	8	on	on	ADP
eurjchem-1252	22	9	a	a	DET
eurjchem-1252	22	10	nicolet	nicolet	PROPN
eurjchem-1252	22	11	6700	6700	NUM
eurjchem-1252	22	12	ft‐ir	ft‐ir	NOUN
eurjchem-1252	22	13	(	(	PUNCT
eurjchem-1252	22	14	thermo	thermo	NOUN
eurjchem-1252	22	15	scientific	scientific	NOUN
eurjchem-1252	22	16	)	)	PUNCT
eurjchem-1252	22	17	as	as	SCONJ
eurjchem-1252	22	18	potassium	potassium	NOUN
eurjchem-1252	22	19	bromide	bromide	NOUN
eurjchem-1252	22	20	pellets	pellet	NOUN
eurjchem-1252	22	21	and	and	CCONJ
eurjchem-1252	22	22	frequencies	frequency	NOUN
eurjchem-1252	22	23	are	be	AUX
eurjchem-1252	22	24	reported	report	VERB
eurjchem-1252	22	25	in	in	ADP
eurjchem-1252	22	26	cm‐1	cm‐1	PROPN
eurjchem-1252	22	27	.	.	PUNCT
eurjchem-1252	23	1	the	the	DET
eurjchem-1252	23	2	mass	mass	ADJ
eurjchem-1252	23	3	spectra	spectra	NOUN
eurjchem-1252	23	4	were	be	AUX
eurjchem-1252	23	5	recorded	record	VERB
eurjchem-1252	23	6	on	on	ADP
eurjchem-1252	23	7	a	a	DET
eurjchem-1252	23	8	gc‐ms	gc‐ms	NOUN
eurjchem-1252	23	9	model	model	NOUN
eurjchem-1252	23	10	shimadzu	shimadzu	ADJ
eurjchem-1252	23	11	qp‐	qp‐	ADV
eurjchem-1252	23	12	2010	2010	NUM
eurjchem-1252	23	13	plus	plus	CCONJ
eurjchem-1252	23	14	ei	ei	ADP
eurjchem-1252	23	15	70	70	NUM
eurjchem-1252	23	16	ev	ev	NOUN
eurjchem-1252	23	17	.	.	PUNCT
eurjchem-1252	24	1	the	the	DET
eurjchem-1252	24	2	1h	1h	NUM
eurjchem-1252	24	3	nmr	nmr	NOUN
eurjchem-1252	24	4	spectra	spectra	NOUN
eurjchem-1252	24	5	were	be	AUX
eurjchem-1252	24	6	recorded	record	VERB
eurjchem-1252	24	7	on	on	ADP
eurjchem-1252	24	8	a	a	DET
eurjchem-1252	24	9	varian	varian	NOUN
eurjchem-1252	24	10	gemini‐300	gemini‐300	PROPN
eurjchem-1252	24	11	mhz	mhz	ADJ
eurjchem-1252	24	12	nmr	nmr	NOUN
eurjchem-1252	24	13	spectrometer	spectrometer	NOUN
eurjchem-1252	24	14	and	and	CCONJ
eurjchem-1252	24	15	chemical	chemical	NOUN
eurjchem-1252	24	16	shifts	shift	NOUN
eurjchem-1252	24	17	δ	δ	PRON
eurjchem-1252	24	18	are	be	AUX
eurjchem-1252	24	19	in	in	ADP
eurjchem-1252	24	20	ppm	ppm	NOUN
eurjchem-1252	24	21	relative	relative	ADJ
eurjchem-1252	24	22	to	to	ADP
eurjchem-1252	24	23	internal	internal	ADJ
eurjchem-1252	24	24	tms	tms	PROPN
eurjchem-1252	24	25	.	.	PUNCT
eurjchem-1252	25	1	reactions	reaction	NOUN
eurjchem-1252	25	2	were	be	AUX
eurjchem-1252	25	3	routinely	routinely	ADV
eurjchem-1252	25	4	followed	follow	VERB
eurjchem-1252	25	5	by	by	ADP
eurjchem-1252	25	6	thin	thin	ADJ
eurjchem-1252	25	7	layer	layer	NOUN
eurjchem-1252	25	8	chromatography	chromatography	NOUN
eurjchem-1252	25	9	(	(	PUNCT
eurjchem-1252	25	10	tlc	tlc	NOUN
eurjchem-1252	25	11	)	)	PUNCT
eurjchem-1252	25	12	on	on	ADP
eurjchem-1252	25	13	silica	silica	NOUN
eurjchem-1252	25	14	gel	gel	NOUN
eurjchem-1252	25	15	;	;	PUNCT
eurjchem-1252	25	16	f254	f254	NUM
eurjchem-1252	25	17	aluminum	aluminum	NOUN
eurjchem-1252	25	18	sheets	sheet	NOUN
eurjchem-1252	25	19	(	(	PUNCT
eurjchem-1252	25	20	merck	merck	NOUN
eurjchem-1252	25	21	)	)	PUNCT
eurjchem-1252	25	22	.	.	PUNCT
eurjchem-1252	26	1	the	the	DET
eurjchem-1252	26	2	spots	spot	NOUN
eurjchem-1252	26	3	were	be	AUX
eurjchem-1252	26	4	detected	detect	VERB
eurjchem-1252	26	5	by	by	ADP
eurjchem-1252	26	6	uv	uv	NOUN
eurjchem-1252	26	7	irradiation	irradiation	NOUN
eurjchem-1252	26	8	at	at	ADP
eurjchem-1252	26	9	254‐365	254‐365	NUM
eurjchem-1252	26	10	nm	nm	NOUN
eurjchem-1252	26	11	.	.	PUNCT
eurjchem-1252	27	1	2.2	2.2	NUM
eurjchem-1252	27	2	.	.	PUNCT
eurjchem-1252	28	1	synthesis	synthesis	NOUN
eurjchem-1252	28	2	2.2.1	2.2.1	NUM
eurjchem-1252	28	3	.	.	PUNCT
eurjchem-1252	28	4	synthesis	synthesis	NOUN
eurjchem-1252	28	5	of	of	ADP
eurjchem-1252	28	6	7,8,9‐triphenyl‐2h‐pyrimido[1,2‐b	7,8,9‐triphenyl‐2h‐pyrimido[1,2‐b	NUM
eurjchem-1252	28	7	]	]	X
eurjchem-1252	28	8	pyridazine‐2,4(3h)‐dione	pyridazine‐2,4(3h)‐dione	NUM
eurjchem-1252	28	9	(	(	PUNCT
eurjchem-1252	28	10	1	1	NUM
eurjchem-1252	28	11	)	)	PUNCT
eurjchem-1252	28	12	a	a	DET
eurjchem-1252	28	13	mixture	mixture	NOUN
eurjchem-1252	28	14	of	of	ADP
eurjchem-1252	28	15	3‐amino‐4,5,6‐triphenylpyridazine	3‐amino‐4,5,6‐triphenylpyridazine	NUM
eurjchem-1252	28	16	[	[	X
eurjchem-1252	28	17	5	5	NUM
eurjchem-1252	28	18	]	]	PUNCT
eurjchem-1252	28	19	(	(	PUNCT
eurjchem-1252	28	20	0.5	0.5	NUM
eurjchem-1252	28	21	g	g	NOUN
eurjchem-1252	28	22	,	,	PUNCT
eurjchem-1252	28	23	1.55	1.55	NUM
eurjchem-1252	28	24	mmol	mmol	NOUN
eurjchem-1252	28	25	)	)	PUNCT
eurjchem-1252	28	26	,	,	PUNCT
eurjchem-1252	28	27	malonic	malonic	ADJ
eurjchem-1252	28	28	acid	acid	NOUN
eurjchem-1252	28	29	(	(	PUNCT
eurjchem-1252	28	30	0.16	0.16	NUM
eurjchem-1252	28	31	g	g	NOUN
eurjchem-1252	28	32	,	,	PUNCT
eurjchem-1252	28	33	1.55	1.55	NUM
eurjchem-1252	28	34	mmol	mmol	NOUN
eurjchem-1252	28	35	)	)	PUNCT
eurjchem-1252	28	36	and	and	CCONJ
eurjchem-1252	28	37	phosphoryl	phosphoryl	PROPN
eurjchem-1252	28	38	chloride	chloride	PROPN
eurjchem-1252	28	39	(	(	PUNCT
eurjchem-1252	28	40	10	10	NUM
eurjchem-1252	28	41	ml	ml	NOUN
eurjchem-1252	28	42	)	)	PUNCT
eurjchem-1252	28	43	was	be	AUX
eurjchem-1252	28	44	heated	heat	VERB
eurjchem-1252	28	45	under	under	ADP
eurjchem-1252	28	46	reflux	reflux	NOUN
eurjchem-1252	28	47	for	for	ADP
eurjchem-1252	28	48	1	1	NUM
eurjchem-1252	28	49	h.	h.	NOUN
eurjchem-1252	28	50	the	the	DET
eurjchem-1252	28	51	reaction	reaction	NOUN
eurjchem-1252	28	52	mixture	mixture	NOUN
eurjchem-1252	28	53	was	be	AUX
eurjchem-1252	28	54	cooled	cool	VERB
eurjchem-1252	28	55	to	to	ADP
eurjchem-1252	28	56	room	room	NOUN
eurjchem-1252	28	57	temperature	temperature	NOUN
eurjchem-1252	28	58	and	and	CCONJ
eurjchem-1252	28	59	poured	pour	VERB
eurjchem-1252	28	60	into	into	ADP
eurjchem-1252	28	61	ice	ice	NOUN
eurjchem-1252	28	62	cooled	cool	VERB
eurjchem-1252	28	63	water	water	NOUN
eurjchem-1252	28	64	(	(	PUNCT
eurjchem-1252	28	65	200	200	NUM
eurjchem-1252	28	66	ml	ml	NOUN
eurjchem-1252	28	67	)	)	PUNCT
eurjchem-1252	28	68	.	.	PUNCT
eurjchem-1252	29	1	deeb	deeb	PROPN
eurjchem-1252	29	2	et	et	PROPN
eurjchem-1252	29	3	al	al	PROPN
eurjchem-1252	29	4	.	.	PUNCT
eurjchem-1252	29	5	/	/	SYM
eurjchem-1252	29	6	european	european	PROPN
eurjchem-1252	29	7	journal	journal	PROPN
eurjchem-1252	29	8	of	of	ADP
eurjchem-1252	29	9	chemistry	chemistry	NOUN
eurjchem-1252	29	10	6	6	NUM
eurjchem-1252	29	11	(	(	PUNCT
eurjchem-1252	29	12	2	2	NUM
eurjchem-1252	29	13	)	)	PUNCT
eurjchem-1252	29	14	(	(	PUNCT
eurjchem-1252	29	15	2015	2015	NUM
eurjchem-1252	29	16	)	)	PUNCT
eurjchem-1252	29	17	204‐210	204‐210	NOUN
eurjchem-1252	29	18	205	205	NUM
eurjchem-1252	29	19	scheme	scheme	NOUN
eurjchem-1252	29	20	1	1	NUM
eurjchem-1252	29	21	the	the	DET
eurjchem-1252	29	22	solid	solid	ADJ
eurjchem-1252	29	23	product	product	NOUN
eurjchem-1252	29	24	was	be	AUX
eurjchem-1252	29	25	filtered	filter	VERB
eurjchem-1252	29	26	off	off	ADP
eurjchem-1252	29	27	,	,	PUNCT
eurjchem-1252	29	28	washed	wash	VERB
eurjchem-1252	29	29	with	with	ADP
eurjchem-1252	29	30	water	water	NOUN
eurjchem-1252	29	31	,	,	PUNCT
eurjchem-1252	29	32	dried	dry	VERB
eurjchem-1252	29	33	and	and	CCONJ
eurjchem-1252	29	34	recrystallized	recrystallize	VERB
eurjchem-1252	29	35	from	from	ADP
eurjchem-1252	29	36	ethanol	ethanol	NOUN
eurjchem-1252	29	37	(	(	PUNCT
eurjchem-1252	29	38	scheme	scheme	NOUN
eurjchem-1252	29	39	1	1	NUM
eurjchem-1252	29	40	)	)	PUNCT
eurjchem-1252	29	41	.	.	PUNCT
eurjchem-1252	30	1	color	color	NOUN
eurjchem-1252	30	2	:	:	PUNCT
eurjchem-1252	30	3	yellow	yellow	ADJ
eurjchem-1252	30	4	.	.	PUNCT
eurjchem-1252	31	1	yield	yield	NOUN
eurjchem-1252	31	2	:	:	PUNCT
eurjchem-1252	31	3	72.70	72.70	NUM
eurjchem-1252	31	4	%	%	NOUN
eurjchem-1252	31	5	.	.	PUNCT
eurjchem-1252	32	1	m.p	m.p	PROPN
eurjchem-1252	32	2	.	.	PROPN
eurjchem-1252	32	3	:	:	PUNCT
eurjchem-1252	33	1	188‐190	188‐190	NUM
eurjchem-1252	33	2	°	°	ADP
eurjchem-1252	33	3	c	c	X
eurjchem-1252	33	4	.	.	PUNCT
eurjchem-1252	34	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	34	2	(	(	PUNCT
eurjchem-1252	34	3	kbr	kbr	PROPN
eurjchem-1252	34	4	,	,	PUNCT
eurjchem-1252	34	5	ν	ν	PROPN
eurjchem-1252	34	6	,	,	PUNCT
eurjchem-1252	34	7	cm‐1	cm‐1	PROPN
eurjchem-1252	34	8	):	):	PUNCT
eurjchem-1252	34	9	3057	3057	NUM
eurjchem-1252	34	10	(	(	PUNCT
eurjchem-1252	34	11	ch	ch	NOUN
eurjchem-1252	34	12	arom	arom	NOUN
eurjchem-1252	34	13	.	.	PUNCT
eurjchem-1252	34	14	)	)	PUNCT
eurjchem-1252	34	15	,	,	PUNCT
eurjchem-1252	34	16	2923	2923	NUM
eurjchem-1252	34	17	(	(	PUNCT
eurjchem-1252	34	18	ch	ch	NOUN
eurjchem-1252	34	19	aliph	aliph	PROPN
eurjchem-1252	34	20	.	.	PUNCT
eurjchem-1252	34	21	)	)	PUNCT
eurjchem-1252	34	22	,	,	PUNCT
eurjchem-1252	34	23	1703	1703	NUM
eurjchem-1252	34	24	(	(	PUNCT
eurjchem-1252	34	25	c	c	NOUN
eurjchem-1252	34	26	=	=	NOUN
eurjchem-1252	34	27	o	o	NOUN
eurjchem-1252	34	28	)	)	PUNCT
eurjchem-1252	34	29	,	,	PUNCT
eurjchem-1252	34	30	1636	1636	NUM
eurjchem-1252	34	31	(	(	PUNCT
eurjchem-1252	34	32	c	c	NOUN
eurjchem-1252	34	33	=	=	SYM
eurjchem-1252	34	34	n	n	NUM
eurjchem-1252	34	35	)	)	PUNCT
eurjchem-1252	34	36	.	.	PUNCT
eurjchem-1252	35	1	1h	1h	NUM
eurjchem-1252	35	2	nmr	nmr	NOUN
eurjchem-1252	35	3	(	(	PUNCT
eurjchem-1252	35	4	300	300	NUM
eurjchem-1252	35	5	mhz	mhz	NOUN
eurjchem-1252	35	6	,	,	PUNCT
eurjchem-1252	35	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1252	35	8	,	,	PUNCT
eurjchem-1252	35	9	δ	δ	PROPN
eurjchem-1252	35	10	,	,	PUNCT
eurjchem-1252	35	11	ppm	ppm	NUM
eurjchem-1252	35	12	):	):	PUNCT
eurjchem-1252	35	13	3.99	3.99	NUM
eurjchem-1252	35	14	(	(	PUNCT
eurjchem-1252	35	15	s	s	PROPN
eurjchem-1252	35	16	,	,	PUNCT
eurjchem-1252	35	17	2h	2h	NUM
eurjchem-1252	35	18	,	,	PUNCT
eurjchem-1252	35	19	ch2	ch2	PROPN
eurjchem-1252	35	20	)	)	PUNCT
eurjchem-1252	35	21	,	,	PUNCT
eurjchem-1252	35	22	6.78‐	6.78‐	NOUN
eurjchem-1252	35	23	7.65	7.65	NUM
eurjchem-1252	35	24	(	(	PUNCT
eurjchem-1252	35	25	m	m	PROPN
eurjchem-1252	35	26	,	,	PUNCT
eurjchem-1252	35	27	15h	15h	NUM
eurjchem-1252	35	28	,	,	PUNCT
eurjchem-1252	35	29	3ph	3ph	NOUN
eurjchem-1252	35	30	)	)	PUNCT
eurjchem-1252	35	31	.	.	PUNCT
eurjchem-1252	36	1	ms	ms	NOUN
eurjchem-1252	36	2	(	(	PUNCT
eurjchem-1252	36	3	ei	ei	PROPN
eurjchem-1252	36	4	,	,	PUNCT
eurjchem-1252	36	5	m	m	PROPN
eurjchem-1252	36	6	/	/	SYM
eurjchem-1252	36	7	z	z	PROPN
eurjchem-1252	36	8	(	(	PUNCT
eurjchem-1252	36	9	%	%	NOUN
eurjchem-1252	36	10	)	)	PUNCT
eurjchem-1252	36	11	):	):	PUNCT
eurjchem-1252	36	12	391	391	NUM
eurjchem-1252	36	13	(	(	PUNCT
eurjchem-1252	36	14	m+	m+	NUM
eurjchem-1252	36	15	,	,	PUNCT
eurjchem-1252	36	16	72.07	72.07	NUM
eurjchem-1252	36	17	)	)	PUNCT
eurjchem-1252	36	18	,	,	PUNCT
eurjchem-1252	36	19	363	363	NUM
eurjchem-1252	36	20	(	(	PUNCT
eurjchem-1252	36	21	11.24	11.24	NUM
eurjchem-1252	36	22	)	)	PUNCT
eurjchem-1252	36	23	,	,	PUNCT
eurjchem-1252	36	24	349	349	NUM
eurjchem-1252	36	25	(	(	PUNCT
eurjchem-1252	36	26	10.60	10.60	NUM
eurjchem-1252	36	27	)	)	PUNCT
eurjchem-1252	36	28	,	,	PUNCT
eurjchem-1252	36	29	335	335	NUM
eurjchem-1252	36	30	(	(	PUNCT
eurjchem-1252	36	31	5.41	5.41	NUM
eurjchem-1252	36	32	)	)	PUNCT
eurjchem-1252	36	33	,	,	PUNCT
eurjchem-1252	36	34	321	321	NUM
eurjchem-1252	36	35	(	(	PUNCT
eurjchem-1252	36	36	16.82	16.82	NUM
eurjchem-1252	36	37	)	)	PUNCT
eurjchem-1252	36	38	,	,	PUNCT
eurjchem-1252	36	39	314	314	NUM
eurjchem-1252	36	40	(	(	PUNCT
eurjchem-1252	36	41	4.59	4.59	NUM
eurjchem-1252	36	42	)	)	PUNCT
eurjchem-1252	36	43	,	,	PUNCT
eurjchem-1252	36	44	288	288	NUM
eurjchem-1252	36	45	(	(	PUNCT
eurjchem-1252	36	46	3.35	3.35	NUM
eurjchem-1252	36	47	)	)	PUNCT
eurjchem-1252	36	48	,	,	PUNCT
eurjchem-1252	36	49	213	213	NUM
eurjchem-1252	36	50	(	(	PUNCT
eurjchem-1252	36	51	3.30	3.30	NUM
eurjchem-1252	36	52	)	)	PUNCT
eurjchem-1252	36	53	,	,	PUNCT
eurjchem-1252	36	54	178	178	NUM
eurjchem-1252	36	55	(	(	PUNCT
eurjchem-1252	36	56	25.40	25.40	NUM
eurjchem-1252	36	57	)	)	PUNCT
eurjchem-1252	36	58	,	,	PUNCT
eurjchem-1252	36	59	103	103	NUM
eurjchem-1252	36	60	(	(	PUNCT
eurjchem-1252	36	61	4.85	4.85	NUM
eurjchem-1252	36	62	)	)	PUNCT
eurjchem-1252	36	63	,	,	PUNCT
eurjchem-1252	36	64	69	69	NUM
eurjchem-1252	36	65	(	(	PUNCT
eurjchem-1252	36	66	100	100	NUM
eurjchem-1252	36	67	)	)	PUNCT
eurjchem-1252	36	68	.	.	PUNCT
eurjchem-1252	37	1	anal	anal	PROPN
eurjchem-1252	37	2	.	.	PUNCT
eurjchem-1252	37	3	calcd	calcd	NOUN
eurjchem-1252	37	4	.	.	PUNCT
eurjchem-1252	38	1	for	for	ADP
eurjchem-1252	38	2	c25h17n3o2	c25h17n3o2	PROPN
eurjchem-1252	38	3	:	:	PUNCT
eurjchem-1252	38	4	c	c	X
eurjchem-1252	38	5	,	,	PUNCT
eurjchem-1252	38	6	76.71	76.71	NUM
eurjchem-1252	38	7	;	;	PUNCT
eurjchem-1252	38	8	h	h	NOUN
eurjchem-1252	38	9	,	,	PUNCT
eurjchem-1252	38	10	4.38	4.38	NUM
eurjchem-1252	38	11	;	;	PUNCT
eurjchem-1252	38	12	n	n	CCONJ
eurjchem-1252	38	13	,	,	PUNCT
eurjchem-1252	38	14	10.74	10.74	NUM
eurjchem-1252	38	15	.	.	PUNCT
eurjchem-1252	38	16	found	find	VERB
eurjchem-1252	38	17	:	:	PUNCT
eurjchem-1252	39	1	c	c	X
eurjchem-1252	39	2	,	,	PUNCT
eurjchem-1252	39	3	76.50	76.50	NUM
eurjchem-1252	39	4	;	;	PUNCT
eurjchem-1252	39	5	h	h	NOUN
eurjchem-1252	39	6	,	,	PUNCT
eurjchem-1252	39	7	4.4.20	4.4.20	NUM
eurjchem-1252	39	8	;	;	PUNCT
eurjchem-1252	39	9	n	n	CCONJ
eurjchem-1252	39	10	,	,	PUNCT
eurjchem-1252	39	11	10.60	10.60	NUM
eurjchem-1252	39	12	%	%	NOUN
eurjchem-1252	39	13	.	.	PUNCT
eurjchem-1252	40	1	2.2.2	2.2.2	X
eurjchem-1252	40	2	.	.	X
eurjchem-1252	41	1	synthesis	synthesis	NOUN
eurjchem-1252	41	2	of	of	ADP
eurjchem-1252	41	3	2‐chloro‐7,8,9‐triphenyl‐4h‐pyrimido	2‐chloro‐7,8,9‐triphenyl‐4h‐pyrimido	NOUN
eurjchem-1252	42	1	[	[	X
eurjchem-1252	42	2	1,2‐b]pyridazin‐4‐one	1,2‐b]pyridazin‐4‐one	NUM
eurjchem-1252	42	3	(	(	PUNCT
eurjchem-1252	42	4	2	2	NUM
eurjchem-1252	42	5	)	)	PUNCT
eurjchem-1252	42	6	a	a	DET
eurjchem-1252	42	7	mixture	mixture	NOUN
eurjchem-1252	42	8	of	of	ADP
eurjchem-1252	42	9	7,8,9‐triphenyl‐2h‐pyrimido[1,2‐b	7,8,9‐triphenyl‐2h‐pyrimido[1,2‐b	NUM
eurjchem-1252	42	10	]	]	PUNCT
eurjchem-1252	42	11	pyridazi	pyridazi	NOUN
eurjchem-1252	42	12	ne‐2,4(3h)‐dione	ne‐2,4(3h)‐dione	NOUN
eurjchem-1252	42	13	(	(	PUNCT
eurjchem-1252	42	14	1	1	NUM
eurjchem-1252	42	15	)	)	PUNCT
eurjchem-1252	42	16	(	(	PUNCT
eurjchem-1252	42	17	0.5	0.5	NUM
eurjchem-1252	42	18	g	g	NOUN
eurjchem-1252	42	19	,	,	PUNCT
eurjchem-1252	42	20	1.28	1.28	NUM
eurjchem-1252	42	21	mmol	mmol	NOUN
eurjchem-1252	42	22	)	)	PUNCT
eurjchem-1252	42	23	and	and	CCONJ
eurjchem-1252	42	24	phosphoryl	phosphoryl	PROPN
eurjchem-1252	42	25	chloride	chloride	PROPN
eurjchem-1252	42	26	(	(	PUNCT
eurjchem-1252	42	27	10	10	NUM
eurjchem-1252	42	28	ml	ml	NOUN
eurjchem-1252	42	29	)	)	PUNCT
eurjchem-1252	42	30	was	be	AUX
eurjchem-1252	42	31	refluxed	refluxe	VERB
eurjchem-1252	42	32	for	for	ADP
eurjchem-1252	42	33	3	3	NUM
eurjchem-1252	42	34	h.	h.	NOUN
eurjchem-1252	42	35	the	the	DET
eurjchem-1252	42	36	reaction	reaction	NOUN
eurjchem-1252	42	37	mixture	mixture	NOUN
eurjchem-1252	42	38	was	be	AUX
eurjchem-1252	42	39	cooled	cool	VERB
eurjchem-1252	42	40	,	,	PUNCT
eurjchem-1252	42	41	poured	pour	VERB
eurjchem-1252	42	42	into	into	ADP
eurjchem-1252	42	43	ice	ice	NOUN
eurjchem-1252	42	44	cold	cold	ADJ
eurjchem-1252	42	45	water	water	NOUN
eurjchem-1252	42	46	(	(	PUNCT
eurjchem-1252	42	47	200	200	NUM
eurjchem-1252	42	48	ml	ml	NOUN
eurjchem-1252	42	49	)	)	PUNCT
eurjchem-1252	42	50	,	,	PUNCT
eurjchem-1252	42	51	and	and	CCONJ
eurjchem-1252	42	52	then	then	ADV
eurjchem-1252	42	53	the	the	DET
eurjchem-1252	42	54	solid	solid	ADJ
eurjchem-1252	42	55	product	product	NOUN
eurjchem-1252	42	56	formed	form	VERB
eurjchem-1252	42	57	was	be	AUX
eurjchem-1252	42	58	filtered	filter	VERB
eurjchem-1252	42	59	off	off	ADP
eurjchem-1252	42	60	,	,	PUNCT
eurjchem-1252	42	61	washed	wash	VERB
eurjchem-1252	42	62	with	with	ADP
eurjchem-1252	42	63	water	water	NOUN
eurjchem-1252	42	64	,	,	PUNCT
eurjchem-1252	42	65	dried	dry	VERB
eurjchem-1252	42	66	,	,	PUNCT
eurjchem-1252	42	67	and	and	CCONJ
eurjchem-1252	42	68	recrystallized	recrystallize	VERB
eurjchem-1252	42	69	from	from	ADP
eurjchem-1252	42	70	ethanol	ethanol	NOUN
eurjchem-1252	42	71	to	to	PART
eurjchem-1252	42	72	give	give	VERB
eurjchem-1252	42	73	compound	compound	NOUN
eurjchem-1252	42	74	2	2	NUM
eurjchem-1252	42	75	(	(	PUNCT
eurjchem-1252	42	76	scheme	scheme	NOUN
eurjchem-1252	42	77	1	1	NUM
eurjchem-1252	42	78	)	)	PUNCT
eurjchem-1252	42	79	.	.	PUNCT
eurjchem-1252	43	1	color	color	NOUN
eurjchem-1252	43	2	:	:	PUNCT
eurjchem-1252	43	3	brown	brown	ADJ
eurjchem-1252	43	4	.	.	PUNCT
eurjchem-1252	44	1	yield	yield	NOUN
eurjchem-1252	44	2	:	:	PUNCT
eurjchem-1252	44	3	84.13	84.13	NUM
eurjchem-1252	44	4	%	%	NOUN
eurjchem-1252	44	5	.	.	PUNCT
eurjchem-1252	45	1	m.p	m.p	PROPN
eurjchem-1252	45	2	.	.	PROPN
eurjchem-1252	45	3	:	:	PUNCT
eurjchem-1252	46	1	226‐228	226‐228	NUM
eurjchem-1252	46	2	°	°	ADP
eurjchem-1252	46	3	c	c	PROPN
eurjchem-1252	46	4	.	.	PUNCT
eurjchem-1252	47	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	47	2	(	(	PUNCT
eurjchem-1252	47	3	kbr	kbr	PROPN
eurjchem-1252	47	4	,	,	PUNCT
eurjchem-1252	47	5	ν	ν	PROPN
eurjchem-1252	47	6	,	,	PUNCT
eurjchem-1252	47	7	cm‐1	cm‐1	PROPN
eurjchem-1252	47	8	):	):	PUNCT
eurjchem-1252	47	9	3057	3057	NUM
eurjchem-1252	47	10	(	(	PUNCT
eurjchem-1252	47	11	c‐h	c‐h	X
eurjchem-1252	47	12	,	,	PUNCT
eurjchem-1252	47	13	arom	arom	NOUN
eurjchem-1252	47	14	.	.	PUNCT
eurjchem-1252	47	15	)	)	PUNCT
eurjchem-1252	47	16	,	,	PUNCT
eurjchem-1252	47	17	1703	1703	NUM
eurjchem-1252	47	18	(	(	PUNCT
eurjchem-1252	47	19	c	c	NOUN
eurjchem-1252	47	20	=	=	NOUN
eurjchem-1252	47	21	o	o	NOUN
eurjchem-1252	47	22	)	)	PUNCT
eurjchem-1252	47	23	,	,	PUNCT
eurjchem-1252	47	24	1638	1638	NUM
eurjchem-1252	47	25	(	(	PUNCT
eurjchem-1252	47	26	c	c	NOUN
eurjchem-1252	47	27	=	=	SYM
eurjchem-1252	47	28	n	n	NUM
eurjchem-1252	47	29	)	)	PUNCT
eurjchem-1252	47	30	.	.	PUNCT
eurjchem-1252	48	1	1h	1h	NUM
eurjchem-1252	48	2	nmr	nmr	NOUN
eurjchem-1252	48	3	(	(	PUNCT
eurjchem-1252	48	4	300	300	NUM
eurjchem-1252	48	5	mhz	mhz	NOUN
eurjchem-1252	48	6	,	,	PUNCT
eurjchem-1252	48	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1252	48	8	,	,	PUNCT
eurjchem-1252	48	9	δ	δ	PROPN
eurjchem-1252	48	10	,	,	PUNCT
eurjchem-1252	48	11	ppm	ppm	NUM
eurjchem-1252	48	12	):	):	PUNCT
eurjchem-1252	48	13	6.65	6.65	NUM
eurjchem-1252	48	14	(	(	PUNCT
eurjchem-1252	48	15	s	s	PROPN
eurjchem-1252	48	16	,	,	PUNCT
eurjchem-1252	48	17	1h	1h	NUM
eurjchem-1252	48	18	,	,	PUNCT
eurjchem-1252	48	19	ch	ch	NOUN
eurjchem-1252	48	20	,	,	PUNCT
eurjchem-1252	48	21	pyrimidine	pyrimidine	NOUN
eurjchem-1252	48	22	ring	ring	NOUN
eurjchem-1252	48	23	)	)	PUNCT
eurjchem-1252	48	24	,	,	PUNCT
eurjchem-1252	48	25	6.78‐7.65	6.78‐7.65	NUM
eurjchem-1252	48	26	(	(	PUNCT
eurjchem-1252	48	27	m	m	PROPN
eurjchem-1252	48	28	,	,	PUNCT
eurjchem-1252	48	29	15h	15h	NUM
eurjchem-1252	48	30	,	,	PUNCT
eurjchem-1252	48	31	3ph	3ph	NOUN
eurjchem-1252	48	32	)	)	PUNCT
eurjchem-1252	48	33	.	.	PUNCT
eurjchem-1252	49	1	ms	ms	NOUN
eurjchem-1252	49	2	(	(	PUNCT
eurjchem-1252	49	3	ei	ei	PROPN
eurjchem-1252	49	4	,	,	PUNCT
eurjchem-1252	49	5	m	m	PROPN
eurjchem-1252	49	6	/	/	SYM
eurjchem-1252	49	7	z	z	PROPN
eurjchem-1252	49	8	(	(	PUNCT
eurjchem-1252	49	9	%	%	NOUN
eurjchem-1252	49	10	)	)	PUNCT
eurjchem-1252	49	11	):	):	PUNCT
eurjchem-1252	49	12	412	412	NUM
eurjchem-1252	49	13	(	(	PUNCT
eurjchem-1252	49	14	m++2	m++2	PROPN
eurjchem-1252	49	15	,	,	PUNCT
eurjchem-1252	49	16	3.50	3.50	NUM
eurjchem-1252	49	17	)	)	PUNCT
eurjchem-1252	49	18	,	,	PUNCT
eurjchem-1252	49	19	410	410	NUM
eurjchem-1252	49	20	(	(	PUNCT
eurjchem-1252	49	21	m+	m+	NUM
eurjchem-1252	49	22	,	,	PUNCT
eurjchem-1252	49	23	51.22	51.22	NUM
eurjchem-1252	49	24	)	)	PUNCT
eurjchem-1252	49	25	,	,	PUNCT
eurjchem-1252	49	26	408	408	NUM
eurjchem-1252	49	27	(	(	PUNCT
eurjchem-1252	49	28	100	100	NUM
eurjchem-1252	49	29	)	)	PUNCT
eurjchem-1252	49	30	,	,	PUNCT
eurjchem-1252	49	31	374	374	NUM
eurjchem-1252	49	32	(	(	PUNCT
eurjchem-1252	49	33	5.13	5.13	NUM
eurjchem-1252	49	34	)	)	PUNCT
eurjchem-1252	49	35	,	,	PUNCT
eurjchem-1252	49	36	369	369	NUM
eurjchem-1252	49	37	(	(	PUNCT
eurjchem-1252	49	38	5.29	5.29	NUM
eurjchem-1252	49	39	)	)	PUNCT
eurjchem-1252	49	40	,	,	PUNCT
eurjchem-1252	49	41	349	349	NUM
eurjchem-1252	49	42	(	(	PUNCT
eurjchem-1252	49	43	5.54	5.54	NUM
eurjchem-1252	49	44	)	)	PUNCT
eurjchem-1252	49	45	,	,	PUNCT
eurjchem-1252	49	46	333	333	NUM
eurjchem-1252	49	47	(	(	PUNCT
eurjchem-1252	49	48	8.63	8.63	NUM
eurjchem-1252	49	49	)	)	PUNCT
eurjchem-1252	49	50	,	,	PUNCT
eurjchem-1252	49	51	307	307	NUM
eurjchem-1252	49	52	(	(	PUNCT
eurjchem-1252	49	53	7.82	7.82	NUM
eurjchem-1252	49	54	)	)	PUNCT
eurjchem-1252	49	55	,	,	PUNCT
eurjchem-1252	49	56	267	267	NUM
eurjchem-1252	49	57	(	(	PUNCT
eurjchem-1252	49	58	9.93	9.93	NUM
eurjchem-1252	49	59	)	)	PUNCT
eurjchem-1252	49	60	,	,	PUNCT
eurjchem-1252	49	61	178	178	NUM
eurjchem-1252	49	62	(	(	PUNCT
eurjchem-1252	49	63	11.32	11.32	NUM
eurjchem-1252	49	64	)	)	PUNCT
eurjchem-1252	49	65	,	,	PUNCT
eurjchem-1252	49	66	103	103	NUM
eurjchem-1252	49	67	(	(	PUNCT
eurjchem-1252	49	68	5.46	5.46	NUM
eurjchem-1252	49	69	)	)	PUNCT
eurjchem-1252	49	70	,	,	PUNCT
eurjchem-1252	49	71	76	76	NUM
eurjchem-1252	49	72	(	(	PUNCT
eurjchem-1252	49	73	9.69	9.69	NUM
eurjchem-1252	49	74	)	)	PUNCT
eurjchem-1252	49	75	,	,	PUNCT
eurjchem-1252	49	76	60	60	NUM
eurjchem-1252	49	77	(	(	PUNCT
eurjchem-1252	49	78	11.07	11.07	NUM
eurjchem-1252	49	79	)	)	PUNCT
eurjchem-1252	49	80	.	.	PUNCT
eurjchem-1252	50	1	anal	anal	PROPN
eurjchem-1252	50	2	.	.	PUNCT
eurjchem-1252	50	3	calcd	calcd	NOUN
eurjchem-1252	50	4	.	.	PUNCT
eurjchem-1252	51	1	for	for	ADP
eurjchem-1252	51	2	c25h16cln3o	c25h16cln3o	NOUN
eurjchem-1252	51	3	:	:	PUNCT
eurjchem-1252	51	4	c	c	X
eurjchem-1252	51	5	,	,	PUNCT
eurjchem-1252	51	6	73.26	73.26	NUM
eurjchem-1252	51	7	;	;	PUNCT
eurjchem-1252	51	8	h	h	NOUN
eurjchem-1252	51	9	,	,	PUNCT
eurjchem-1252	51	10	3.93	3.93	NUM
eurjchem-1252	51	11	;	;	PUNCT
eurjchem-1252	51	12	n	n	CCONJ
eurjchem-1252	51	13	,	,	PUNCT
eurjchem-1252	51	14	10.25	10.25	NUM
eurjchem-1252	51	15	.	.	PUNCT
eurjchem-1252	51	16	found	find	VERB
eurjchem-1252	51	17	:	:	PUNCT
eurjchem-1252	52	1	c	c	X
eurjchem-1252	52	2	,	,	PUNCT
eurjchem-1252	52	3	73.59	73.59	NUM
eurjchem-1252	52	4	;	;	PUNCT
eurjchem-1252	52	5	h	h	NOUN
eurjchem-1252	52	6	,	,	PUNCT
eurjchem-1252	52	7	3.78	3.78	NUM
eurjchem-1252	52	8	;	;	PUNCT
eurjchem-1252	52	9	n	n	CCONJ
eurjchem-1252	52	10	,	,	PUNCT
eurjchem-1252	52	11	10.52	10.52	NUM
eurjchem-1252	52	12	%	%	NOUN
eurjchem-1252	52	13	.	.	PUNCT
eurjchem-1252	53	1	2.2.3	2.2.3	X
eurjchem-1252	53	2	.	.	X
eurjchem-1252	54	1	synthesis	synthesis	NOUN
eurjchem-1252	54	2	of	of	ADP
eurjchem-1252	54	3	2‐methoxy‐7,8,9‐triphenyl‐4h‐pyrimido	2‐methoxy‐7,8,9‐triphenyl‐4h‐pyrimido	PRON
eurjchem-1252	55	1	[	[	X
eurjchem-1252	55	2	1,2‐b]pyridazin‐4‐one	1,2‐b]pyridazin‐4‐one	NUM
eurjchem-1252	55	3	(	(	PUNCT
eurjchem-1252	55	4	3a	3a	NUM
eurjchem-1252	55	5	)	)	PUNCT
eurjchem-1252	55	6	compound	compound	NOUN
eurjchem-1252	55	7	2	2	NUM
eurjchem-1252	55	8	(	(	PUNCT
eurjchem-1252	55	9	0.5	0.5	NUM
eurjchem-1252	55	10	g	g	NOUN
eurjchem-1252	55	11	,	,	PUNCT
eurjchem-1252	55	12	1.22	1.22	NUM
eurjchem-1252	55	13	mmol	mmol	NOUN
eurjchem-1252	55	14	)	)	PUNCT
eurjchem-1252	55	15	was	be	AUX
eurjchem-1252	55	16	added	add	VERB
eurjchem-1252	55	17	to	to	ADP
eurjchem-1252	55	18	a	a	DET
eurjchem-1252	55	19	solution	solution	NOUN
eurjchem-1252	55	20	of	of	ADP
eurjchem-1252	55	21	sodium	sodium	NOUN
eurjchem-1252	55	22	methoxide	methoxide	NOUN
eurjchem-1252	55	23	(	(	PUNCT
eurjchem-1252	55	24	0.1	0.1	NUM
eurjchem-1252	55	25	g	g	NOUN
eurjchem-1252	55	26	of	of	ADP
eurjchem-1252	55	27	na	na	INTJ
eurjchem-1252	55	28	in	in	ADP
eurjchem-1252	55	29	10	10	NUM
eurjchem-1252	55	30	ml	ml	NOUN
eurjchem-1252	55	31	of	of	ADP
eurjchem-1252	55	32	pure	pure	ADJ
eurjchem-1252	55	33	methanol	methanol	NOUN
eurjchem-1252	55	34	)	)	PUNCT
eurjchem-1252	55	35	.	.	PUNCT
eurjchem-1252	56	1	the	the	DET
eurjchem-1252	56	2	reaction	reaction	NOUN
eurjchem-1252	56	3	mixture	mixture	NOUN
eurjchem-1252	56	4	was	be	AUX
eurjchem-1252	56	5	refluxed	refluxe	VERB
eurjchem-1252	56	6	for	for	ADP
eurjchem-1252	56	7	3	3	NUM
eurjchem-1252	56	8	h.	h.	NOUN
eurjchem-1252	56	9	the	the	DET
eurjchem-1252	56	10	solvent	solvent	NOUN
eurjchem-1252	56	11	was	be	AUX
eurjchem-1252	56	12	concentrated	concentrate	VERB
eurjchem-1252	56	13	,	,	PUNCT
eurjchem-1252	56	14	and	and	CCONJ
eurjchem-1252	56	15	then	then	ADV
eurjchem-1252	56	16	the	the	DET
eurjchem-1252	56	17	solid	solid	ADJ
eurjchem-1252	56	18	product	product	NOUN
eurjchem-1252	56	19	was	be	AUX
eurjchem-1252	56	20	filtered	filter	VERB
eurjchem-1252	56	21	off	off	ADP
eurjchem-1252	56	22	,	,	PUNCT
eurjchem-1252	56	23	dried	dry	VERB
eurjchem-1252	56	24	,	,	PUNCT
eurjchem-1252	56	25	and	and	CCONJ
eurjchem-1252	56	26	recrystallized	recrystallize	VERB
eurjchem-1252	56	27	from	from	ADP
eurjchem-1252	56	28	ethanol	ethanol	NOUN
eurjchem-1252	56	29	to	to	PART
eurjchem-1252	56	30	give	give	VERB
eurjchem-1252	56	31	compound	compound	NOUN
eurjchem-1252	56	32	3a	3a	PROPN
eurjchem-1252	56	33	(	(	PUNCT
eurjchem-1252	56	34	scheme	scheme	NOUN
eurjchem-1252	56	35	1	1	NUM
eurjchem-1252	56	36	)	)	PUNCT
eurjchem-1252	56	37	.	.	PUNCT
eurjchem-1252	57	1	color	color	NOUN
eurjchem-1252	57	2	:	:	PUNCT
eurjchem-1252	57	3	brown	brown	ADJ
eurjchem-1252	57	4	crystals	crystal	NOUN
eurjchem-1252	57	5	.	.	PUNCT
eurjchem-1252	58	1	yield	yield	NOUN
eurjchem-1252	58	2	:	:	PUNCT
eurjchem-1252	58	3	74.75	74.75	NUM
eurjchem-1252	58	4	%	%	NOUN
eurjchem-1252	58	5	.	.	PUNCT
eurjchem-1252	59	1	m.p	m.p	PROPN
eurjchem-1252	59	2	.	.	PROPN
eurjchem-1252	59	3	:	:	PUNCT
eurjchem-1252	60	1	146‐	146‐	NUM
eurjchem-1252	60	2	148	148	NUM
eurjchem-1252	60	3	°	°	SYM
eurjchem-1252	60	4	c	c	NOUN
eurjchem-1252	60	5	.	.	PUNCT
eurjchem-1252	61	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	61	2	(	(	PUNCT
eurjchem-1252	61	3	kbr	kbr	PROPN
eurjchem-1252	61	4	,	,	PUNCT
eurjchem-1252	61	5	ν	ν	PROPN
eurjchem-1252	61	6	,	,	PUNCT
eurjchem-1252	61	7	cm‐1	cm‐1	PROPN
eurjchem-1252	61	8	):	):	PUNCT
eurjchem-1252	61	9	3056	3056	NUM
eurjchem-1252	61	10	(	(	PUNCT
eurjchem-1252	61	11	c‐h	c‐h	X
eurjchem-1252	61	12	,	,	PUNCT
eurjchem-1252	61	13	arom	arom	NOUN
eurjchem-1252	61	14	.	.	PUNCT
eurjchem-1252	61	15	)	)	PUNCT
eurjchem-1252	61	16	,	,	PUNCT
eurjchem-1252	61	17	2927	2927	NUM
eurjchem-1252	61	18	(	(	PUNCT
eurjchem-1252	61	19	c‒h	c‒h	PROPN
eurjchem-1252	61	20	,	,	PUNCT
eurjchem-1252	61	21	aliph	aliph	NOUN
eurjchem-1252	61	22	.	.	PUNCT
eurjchem-1252	61	23	)	)	PUNCT
eurjchem-1252	61	24	,	,	PUNCT
eurjchem-1252	61	25	1705	1705	NUM
eurjchem-1252	61	26	(	(	PUNCT
eurjchem-1252	61	27	c	c	NOUN
eurjchem-1252	61	28	=	=	NOUN
eurjchem-1252	61	29	o	o	NOUN
eurjchem-1252	61	30	)	)	PUNCT
eurjchem-1252	61	31	,	,	PUNCT
eurjchem-1252	61	32	1645	1645	NUM
eurjchem-1252	61	33	(	(	PUNCT
eurjchem-1252	61	34	c	c	NOUN
eurjchem-1252	61	35	=	=	SYM
eurjchem-1252	61	36	n	n	NUM
eurjchem-1252	61	37	)	)	PUNCT
eurjchem-1252	61	38	.	.	PUNCT
eurjchem-1252	62	1	1h	1h	NUM
eurjchem-1252	62	2	nmr	nmr	NOUN
eurjchem-1252	62	3	(	(	PUNCT
eurjchem-1252	62	4	300	300	NUM
eurjchem-1252	62	5	mhz	mhz	NOUN
eurjchem-1252	62	6	,	,	PUNCT
eurjchem-1252	62	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1252	62	8	,	,	PUNCT
eurjchem-1252	62	9	δ	δ	PROPN
eurjchem-1252	62	10	,	,	PUNCT
eurjchem-1252	62	11	ppm	ppm	NUM
eurjchem-1252	62	12	):	):	PUNCT
eurjchem-1252	62	13	5.66	5.66	NUM
eurjchem-1252	62	14	(	(	PUNCT
eurjchem-1252	62	15	s	s	PROPN
eurjchem-1252	62	16	,	,	PUNCT
eurjchem-1252	62	17	3h	3h	NUM
eurjchem-1252	62	18	,	,	PUNCT
eurjchem-1252	62	19	ch3	ch3	PROPN
eurjchem-1252	62	20	)	)	PUNCT
eurjchem-1252	62	21	,	,	PUNCT
eurjchem-1252	62	22	5.87	5.87	NUM
eurjchem-1252	62	23	(	(	PUNCT
eurjchem-1252	62	24	s	s	PROPN
eurjchem-1252	62	25	,	,	PUNCT
eurjchem-1252	62	26	1h	1h	NUM
eurjchem-1252	62	27	,	,	PUNCT
eurjchem-1252	62	28	ch	ch	NOUN
eurjchem-1252	62	29	,	,	PUNCT
eurjchem-1252	62	30	pyrimidine	pyrimidine	NOUN
eurjchem-1252	62	31	ring	ring	NOUN
eurjchem-1252	62	32	)	)	PUNCT
eurjchem-1252	62	33	,	,	PUNCT
eurjchem-1252	62	34	6.89‐7.65	6.89‐7.65	NUM
eurjchem-1252	62	35	(	(	PUNCT
eurjchem-1252	62	36	m	m	PROPN
eurjchem-1252	62	37	,	,	PUNCT
eurjchem-1252	62	38	15h	15h	NUM
eurjchem-1252	62	39	,	,	PUNCT
eurjchem-1252	62	40	3ph	3ph	NOUN
eurjchem-1252	62	41	)	)	PUNCT
eurjchem-1252	62	42	.	.	PUNCT
eurjchem-1252	63	1	ms	ms	NOUN
eurjchem-1252	63	2	(	(	PUNCT
eurjchem-1252	63	3	ei	ei	PROPN
eurjchem-1252	63	4	,	,	PUNCT
eurjchem-1252	63	5	m	m	PROPN
eurjchem-1252	63	6	/	/	SYM
eurjchem-1252	63	7	z	z	PROPN
eurjchem-1252	63	8	(	(	PUNCT
eurjchem-1252	63	9	%	%	NOUN
eurjchem-1252	63	10	)	)	PUNCT
eurjchem-1252	63	11	):	):	PUNCT
eurjchem-1252	63	12	405	405	NUM
eurjchem-1252	63	13	(	(	PUNCT
eurjchem-1252	63	14	m+	m+	NUM
eurjchem-1252	63	15	,	,	PUNCT
eurjchem-1252	63	16	96.55	96.55	NUM
eurjchem-1252	63	17	)	)	PUNCT
eurjchem-1252	63	18	,	,	PUNCT
eurjchem-1252	63	19	390	390	NUM
eurjchem-1252	63	20	(	(	PUNCT
eurjchem-1252	63	21	72.41	72.41	NUM
eurjchem-1252	63	22	)	)	PUNCT
eurjchem-1252	63	23	,	,	PUNCT
eurjchem-1252	63	24	376	376	NUM
eurjchem-1252	63	25	(	(	PUNCT
eurjchem-1252	63	26	75.86	75.86	NUM
eurjchem-1252	63	27	)	)	PUNCT
eurjchem-1252	63	28	,	,	PUNCT
eurjchem-1252	63	29	349	349	NUM
eurjchem-1252	63	30	(	(	PUNCT
eurjchem-1252	63	31	81.61	81.61	NUM
eurjchem-1252	63	32	)	)	PUNCT
eurjchem-1252	63	33	,	,	PUNCT
eurjchem-1252	63	34	334	334	NUM
eurjchem-1252	63	35	(	(	PUNCT
eurjchem-1252	63	36	59.77	59.77	NUM
eurjchem-1252	63	37	)	)	PUNCT
eurjchem-1252	63	38	,	,	PUNCT
eurjchem-1252	63	39	200	200	NUM
eurjchem-1252	63	40	(	(	PUNCT
eurjchem-1252	63	41	100	100	NUM
eurjchem-1252	63	42	)	)	PUNCT
eurjchem-1252	63	43	,	,	PUNCT
eurjchem-1252	63	44	71	71	NUM
eurjchem-1252	63	45	(	(	PUNCT
eurjchem-1252	63	46	75.86	75.86	NUM
eurjchem-1252	63	47	)	)	PUNCT
eurjchem-1252	63	48	,	,	PUNCT
eurjchem-1252	63	49	57	57	NUM
eurjchem-1252	63	50	(	(	PUNCT
eurjchem-1252	63	51	31.03	31.03	NUM
eurjchem-1252	63	52	)	)	PUNCT
eurjchem-1252	63	53	.	.	PUNCT
eurjchem-1252	64	1	anal	anal	PROPN
eurjchem-1252	64	2	.	.	PUNCT
eurjchem-1252	64	3	calcd	calcd	NOUN
eurjchem-1252	64	4	.	.	PUNCT
eurjchem-1252	65	1	for	for	ADP
eurjchem-1252	65	2	c26h19n3o2	c26h19n3o2	PROPN
eurjchem-1252	65	3	:	:	PUNCT
eurjchem-1252	65	4	c	c	X
eurjchem-1252	65	5	,	,	PUNCT
eurjchem-1252	65	6	77.02	77.02	NUM
eurjchem-1252	65	7	;	;	PUNCT
eurjchem-1252	65	8	h	h	NOUN
eurjchem-1252	65	9	,	,	PUNCT
eurjchem-1252	65	10	4.72	4.72	NUM
eurjchem-1252	65	11	;	;	PUNCT
eurjchem-1252	65	12	n	n	CCONJ
eurjchem-1252	65	13	,	,	PUNCT
eurjchem-1252	65	14	10.36	10.36	NUM
eurjchem-1252	65	15	.	.	PUNCT
eurjchem-1252	66	1	found	find	VERB
eurjchem-1252	66	2	:	:	PUNCT
eurjchem-1252	67	1	c	c	X
eurjchem-1252	67	2	,	,	PUNCT
eurjchem-1252	67	3	77.39	77.39	NUM
eurjchem-1252	67	4	;	;	PUNCT
eurjchem-1252	67	5	h	h	NOUN
eurjchem-1252	67	6	,	,	PUNCT
eurjchem-1252	67	7	4.53	4.53	NUM
eurjchem-1252	67	8	;	;	PUNCT
eurjchem-1252	67	9	n	n	CCONJ
eurjchem-1252	67	10	,	,	PUNCT
eurjchem-1252	67	11	10.62	10.62	NUM
eurjchem-1252	67	12	%	%	NOUN
eurjchem-1252	67	13	.	.	PUNCT
eurjchem-1252	68	1	2.2.4	2.2.4	X
eurjchem-1252	68	2	.	.	X
eurjchem-1252	68	3	synthesis	synthesis	NOUN
eurjchem-1252	68	4	of	of	ADP
eurjchem-1252	68	5	2‐ethoxy‐7,8,9‐triphenyl‐4h‐pyrimido	2‐ethoxy‐7,8,9‐triphenyl‐4h‐pyrimido	NUM
eurjchem-1252	69	1	[	[	X
eurjchem-1252	69	2	1,2‐b]pyridazin‐4‐one	1,2‐b]pyridazin‐4‐one	NUM
eurjchem-1252	69	3	(	(	PUNCT
eurjchem-1252	69	4	3b	3b	NUM
eurjchem-1252	69	5	)	)	PUNCT
eurjchem-1252	69	6	compound	compound	NOUN
eurjchem-1252	69	7	2	2	NUM
eurjchem-1252	69	8	(	(	PUNCT
eurjchem-1252	69	9	0.5	0.5	NUM
eurjchem-1252	69	10	g	g	NOUN
eurjchem-1252	69	11	,	,	PUNCT
eurjchem-1252	69	12	1.22	1.22	NUM
eurjchem-1252	69	13	mmol	mmol	NOUN
eurjchem-1252	69	14	)	)	PUNCT
eurjchem-1252	69	15	was	be	AUX
eurjchem-1252	69	16	added	add	VERB
eurjchem-1252	69	17	to	to	ADP
eurjchem-1252	69	18	a	a	DET
eurjchem-1252	69	19	solution	solution	NOUN
eurjchem-1252	69	20	of	of	ADP
eurjchem-1252	69	21	sodium	sodium	NOUN
eurjchem-1252	69	22	ethoxide	ethoxide	NOUN
eurjchem-1252	69	23	(	(	PUNCT
eurjchem-1252	69	24	0.1	0.1	NUM
eurjchem-1252	69	25	g	g	NOUN
eurjchem-1252	69	26	of	of	ADP
eurjchem-1252	69	27	na	na	INTJ
eurjchem-1252	69	28	in	in	ADP
eurjchem-1252	69	29	10	10	NUM
eurjchem-1252	69	30	ml	ml	NOUN
eurjchem-1252	69	31	of	of	ADP
eurjchem-1252	69	32	absolute	absolute	ADJ
eurjchem-1252	69	33	ethanol	ethanol	NOUN
eurjchem-1252	69	34	)	)	PUNCT
eurjchem-1252	69	35	.	.	PUNCT
eurjchem-1252	70	1	the	the	DET
eurjchem-1252	70	2	reaction	reaction	NOUN
eurjchem-1252	70	3	mixture	mixture	NOUN
eurjchem-1252	70	4	was	be	AUX
eurjchem-1252	70	5	refluxed	refluxe	VERB
eurjchem-1252	70	6	for	for	ADP
eurjchem-1252	70	7	3	3	NUM
eurjchem-1252	70	8	h.	h.	NOUN
eurjchem-1252	70	9	the	the	DET
eurjchem-1252	70	10	solvent	solvent	NOUN
eurjchem-1252	70	11	was	be	AUX
eurjchem-1252	70	12	concentrated	concentrate	VERB
eurjchem-1252	70	13	;	;	PUNCT
eurjchem-1252	70	14	and	and	CCONJ
eurjchem-1252	70	15	then	then	ADV
eurjchem-1252	70	16	the	the	DET
eurjchem-1252	70	17	solid	solid	ADJ
eurjchem-1252	70	18	product	product	NOUN
eurjchem-1252	70	19	was	be	AUX
eurjchem-1252	70	20	filtered	filter	VERB
eurjchem-1252	70	21	off	off	ADP
eurjchem-1252	70	22	,	,	PUNCT
eurjchem-1252	70	23	dried	dry	VERB
eurjchem-1252	70	24	,	,	PUNCT
eurjchem-1252	70	25	and	and	CCONJ
eurjchem-1252	70	26	recrystallized	recrystallize	VERB
eurjchem-1252	70	27	from	from	ADP
eurjchem-1252	70	28	ethanol	ethanol	NOUN
eurjchem-1252	70	29	to	to	PART
eurjchem-1252	70	30	give	give	VERB
eurjchem-1252	70	31	compound	compound	NOUN
eurjchem-1252	70	32	3b	3b	NOUN
eurjchem-1252	70	33	(	(	PUNCT
eurjchem-1252	70	34	scheme	scheme	NOUN
eurjchem-1252	70	35	1	1	NUM
eurjchem-1252	70	36	)	)	PUNCT
eurjchem-1252	70	37	.	.	PUNCT
eurjchem-1252	71	1	color	color	NOUN
eurjchem-1252	71	2	:	:	PUNCT
eurjchem-1252	71	3	brown	brown	ADJ
eurjchem-1252	71	4	.	.	PUNCT
eurjchem-1252	72	1	yield	yield	NOUN
eurjchem-1252	72	2	:	:	PUNCT
eurjchem-1252	72	3	74.26	74.26	NUM
eurjchem-1252	72	4	%	%	NOUN
eurjchem-1252	72	5	.	.	PUNCT
eurjchem-1252	73	1	m.p	m.p	PROPN
eurjchem-1252	73	2	.	.	PROPN
eurjchem-1252	73	3	:	:	PUNCT
eurjchem-1252	74	1	200‐205	200‐205	NUM
eurjchem-1252	74	2	°	°	ADP
eurjchem-1252	74	3	c	c	X
eurjchem-1252	74	4	.	.	PUNCT
eurjchem-1252	74	5	ft‐ir	ft‐ir	NOUN
eurjchem-1252	74	6	(	(	PUNCT
eurjchem-1252	74	7	kbr	kbr	PROPN
eurjchem-1252	74	8	,	,	PUNCT
eurjchem-1252	74	9	ν	ν	PROPN
eurjchem-1252	74	10	,	,	PUNCT
eurjchem-1252	74	11	cm‐1	cm‐1	PROPN
eurjchem-1252	74	12	):	):	PUNCT
eurjchem-1252	74	13	3058	3058	NUM
eurjchem-1252	74	14	(	(	PUNCT
eurjchem-1252	74	15	ch	ch	NOUN
eurjchem-1252	74	16	,	,	PUNCT
eurjchem-1252	74	17	arom	arom	NOUN
eurjchem-1252	74	18	.	.	PUNCT
eurjchem-1252	74	19	)	)	PUNCT
eurjchem-1252	74	20	,	,	PUNCT
eurjchem-1252	74	21	2975	2975	NUM
eurjchem-1252	74	22	,	,	PUNCT
eurjchem-1252	74	23	2924	2924	NUM
eurjchem-1252	74	24	(	(	PUNCT
eurjchem-1252	74	25	ch	ch	NOUN
eurjchem-1252	74	26	,	,	PUNCT
eurjchem-1252	74	27	aliph	aliph	NOUN
eurjchem-1252	74	28	.	.	PUNCT
eurjchem-1252	74	29	)	)	PUNCT
eurjchem-1252	75	1	,	,	PUNCT
eurjchem-1252	75	2	1695	1695	NUM
eurjchem-1252	75	3	(	(	PUNCT
eurjchem-1252	75	4	c	c	NOUN
eurjchem-1252	75	5	=	=	NOUN
eurjchem-1252	75	6	o	o	NOUN
eurjchem-1252	75	7	)	)	PUNCT
eurjchem-1252	75	8	,	,	PUNCT
eurjchem-1252	75	9	1643	1643	NUM
eurjchem-1252	75	10	(	(	PUNCT
eurjchem-1252	75	11	c	c	NOUN
eurjchem-1252	75	12	=	=	SYM
eurjchem-1252	75	13	n	n	NUM
eurjchem-1252	75	14	)	)	PUNCT
eurjchem-1252	75	15	,	,	PUNCT
eurjchem-1252	75	16	1234	1234	NUM
eurjchem-1252	75	17	(	(	PUNCT
eurjchem-1252	75	18	c‒o	c‒o	PROPN
eurjchem-1252	75	19	)	)	PUNCT
eurjchem-1252	75	20	.	.	PUNCT
eurjchem-1252	76	1	1h	1h	NUM
eurjchem-1252	76	2	nmr	nmr	NOUN
eurjchem-1252	76	3	(	(	PUNCT
eurjchem-1252	76	4	300	300	NUM
eurjchem-1252	76	5	mhz	mhz	NOUN
eurjchem-1252	76	6	,	,	PUNCT
eurjchem-1252	76	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1252	76	8	,	,	PUNCT
eurjchem-1252	76	9	δ	δ	PROPN
eurjchem-1252	76	10	,	,	PUNCT
eurjchem-1252	76	11	ppm	ppm	NUM
eurjchem-1252	76	12	):	):	PUNCT
eurjchem-1252	76	13	1.14	1.14	NUM
eurjchem-1252	76	14	(	(	PUNCT
eurjchem-1252	76	15	t	t	PROPN
eurjchem-1252	76	16	,	,	PUNCT
eurjchem-1252	76	17	3h	3h	NUM
eurjchem-1252	76	18	,	,	PUNCT
eurjchem-1252	76	19	ch2ch3	ch2ch3	ADJ
eurjchem-1252	76	20	)	)	PUNCT
eurjchem-1252	76	21	,	,	PUNCT
eurjchem-1252	76	22	4.05	4.05	NUM
eurjchem-1252	76	23	(	(	PUNCT
eurjchem-1252	76	24	q	q	NOUN
eurjchem-1252	76	25	,	,	PUNCT
eurjchem-1252	76	26	2h	2h	NUM
eurjchem-1252	76	27	,	,	PUNCT
eurjchem-1252	76	28	ch2ch3	ch2ch3	ADJ
eurjchem-1252	76	29	)	)	PUNCT
eurjchem-1252	76	30	,	,	PUNCT
eurjchem-1252	76	31	5.67	5.67	NUM
eurjchem-1252	76	32	(	(	PUNCT
eurjchem-1252	76	33	s	s	PROPN
eurjchem-1252	76	34	,	,	PUNCT
eurjchem-1252	76	35	1h	1h	NUM
eurjchem-1252	76	36	,	,	PUNCT
eurjchem-1252	76	37	ch	ch	NOUN
eurjchem-1252	76	38	,	,	PUNCT
eurjchem-1252	76	39	pyrimidine	pyrimidine	NOUN
eurjchem-1252	76	40	ring	ring	NOUN
eurjchem-1252	76	41	)	)	PUNCT
eurjchem-1252	76	42	,	,	PUNCT
eurjchem-1252	76	43	6.94‐7.65	6.94‐7.65	NUM
eurjchem-1252	76	44	(	(	PUNCT
eurjchem-1252	76	45	m	m	PROPN
eurjchem-1252	76	46	,	,	PUNCT
eurjchem-1252	76	47	15h	15h	NUM
eurjchem-1252	76	48	,	,	PUNCT
eurjchem-1252	76	49	3ph	3ph	NOUN
eurjchem-1252	76	50	)	)	PUNCT
eurjchem-1252	76	51	.	.	PUNCT
eurjchem-1252	77	1	ms	ms	NOUN
eurjchem-1252	77	2	(	(	PUNCT
eurjchem-1252	77	3	ei	ei	PROPN
eurjchem-1252	77	4	,	,	PUNCT
eurjchem-1252	77	5	m	m	PROPN
eurjchem-1252	77	6	/	/	SYM
eurjchem-1252	77	7	z	z	PROPN
eurjchem-1252	77	8	(	(	PUNCT
eurjchem-1252	77	9	%	%	NOUN
eurjchem-1252	77	10	)	)	PUNCT
eurjchem-1252	77	11	):	):	PUNCT
eurjchem-1252	77	12	419	419	NUM
eurjchem-1252	77	13	(	(	PUNCT
eurjchem-1252	77	14	m+	m+	NUM
eurjchem-1252	77	15	,	,	PUNCT
eurjchem-1252	77	16	14.45	14.45	NUM
eurjchem-1252	77	17	)	)	PUNCT
eurjchem-1252	77	18	,	,	PUNCT
eurjchem-1252	77	19	404	404	NUM
eurjchem-1252	77	20	(	(	PUNCT
eurjchem-1252	77	21	7.00	7.00	NUM
eurjchem-1252	77	22	)	)	PUNCT
eurjchem-1252	77	23	,	,	PUNCT
eurjchem-1252	77	24	390	390	NUM
eurjchem-1252	77	25	(	(	PUNCT
eurjchem-1252	77	26	23.58	23.58	NUM
eurjchem-1252	77	27	)	)	PUNCT
eurjchem-1252	77	28	,	,	PUNCT
eurjchem-1252	77	29	322	322	NUM
eurjchem-1252	77	30	(	(	PUNCT
eurjchem-1252	77	31	100	100	NUM
eurjchem-1252	77	32	)	)	PUNCT
eurjchem-1252	77	33	,	,	PUNCT
eurjchem-1252	77	34	307	307	NUM
eurjchem-1252	77	35	(	(	PUNCT
eurjchem-1252	77	36	4.01	4.01	NUM
eurjchem-1252	77	37	)	)	PUNCT
eurjchem-1252	77	38	,	,	PUNCT
eurjchem-1252	77	39	178	178	NUM
eurjchem-1252	77	40	(	(	PUNCT
eurjchem-1252	77	41	18.86	18.86	NUM
eurjchem-1252	77	42	)	)	PUNCT
eurjchem-1252	77	43	,	,	PUNCT
eurjchem-1252	77	44	138	138	NUM
eurjchem-1252	77	45	(	(	PUNCT
eurjchem-1252	77	46	4.78	4.78	NUM
eurjchem-1252	77	47	)	)	PUNCT
eurjchem-1252	77	48	,	,	PUNCT
eurjchem-1252	77	49	77	77	NUM
eurjchem-1252	77	50	(	(	PUNCT
eurjchem-1252	77	51	43.56	43.56	NUM
eurjchem-1252	77	52	)	)	PUNCT
eurjchem-1252	77	53	.	.	PUNCT
eurjchem-1252	78	1	anal	anal	PROPN
eurjchem-1252	78	2	.	.	PUNCT
eurjchem-1252	78	3	calcd	calcd	NOUN
eurjchem-1252	78	4	.	.	PUNCT
eurjchem-1252	79	1	for	for	SCONJ
eurjchem-1252	79	2	c27h21n3o2	c27h21n3o2	PROPN
eurjchem-1252	79	3	:	:	PUNCT
eurjchem-1252	79	4	c	c	X
eurjchem-1252	79	5	,	,	PUNCT
eurjchem-1252	79	6	77.31	77.31	NUM
eurjchem-1252	79	7	;	;	PUNCT
eurjchem-1252	79	8	h	h	NOUN
eurjchem-1252	79	9	,	,	PUNCT
eurjchem-1252	79	10	5.05	5.05	NUM
eurjchem-1252	79	11	;	;	PUNCT
eurjchem-1252	79	12	n	n	CCONJ
eurjchem-1252	79	13	,	,	PUNCT
eurjchem-1252	79	14	10.02	10.02	NUM
eurjchem-1252	79	15	.	.	PUNCT
eurjchem-1252	79	16	found	find	VERB
eurjchem-1252	79	17	:	:	PUNCT
eurjchem-1252	80	1	c	c	X
eurjchem-1252	80	2	,	,	PUNCT
eurjchem-1252	80	3	77.67	77.67	NUM
eurjchem-1252	80	4	;	;	PUNCT
eurjchem-1252	80	5	h	h	NOUN
eurjchem-1252	80	6	,	,	PUNCT
eurjchem-1252	80	7	4.88	4.88	NUM
eurjchem-1252	80	8	;	;	PUNCT
eurjchem-1252	80	9	n	n	CCONJ
eurjchem-1252	80	10	,	,	PUNCT
eurjchem-1252	80	11	10.25	10.25	NUM
eurjchem-1252	80	12	%	%	NOUN
eurjchem-1252	80	13	.	.	PUNCT
eurjchem-1252	81	1	2.2.5	2.2.5	X
eurjchem-1252	81	2	.	.	X
eurjchem-1252	81	3	synthesis	synthesis	NOUN
eurjchem-1252	81	4	of	of	ADP
eurjchem-1252	81	5	2‐azido‐7,8,9‐triphenyl‐4h‐pyrimido[1,2‐	2‐azido‐7,8,9‐triphenyl‐4h‐pyrimido[1,2‐	NUM
eurjchem-1252	81	6	b]pyridazin‐4‐one	b]pyridazin‐4‐one	NOUN
eurjchem-1252	81	7	(	(	PUNCT
eurjchem-1252	81	8	3c	3c	NUM
eurjchem-1252	81	9	)	)	PUNCT
eurjchem-1252	81	10	a	a	DET
eurjchem-1252	81	11	solution	solution	NOUN
eurjchem-1252	81	12	of	of	ADP
eurjchem-1252	81	13	compound	compound	NOUN
eurjchem-1252	81	14	2	2	NUM
eurjchem-1252	81	15	(	(	PUNCT
eurjchem-1252	81	16	0.5	0.5	NUM
eurjchem-1252	81	17	g	g	NOUN
eurjchem-1252	81	18	,	,	PUNCT
eurjchem-1252	81	19	1.22	1.22	NUM
eurjchem-1252	81	20	mmol	mmol	NOUN
eurjchem-1252	81	21	)	)	PUNCT
eurjchem-1252	81	22	,	,	PUNCT
eurjchem-1252	81	23	and	and	CCONJ
eurjchem-1252	81	24	sodium	sodium	NOUN
eurjchem-1252	81	25	azide	azide	NOUN
eurjchem-1252	81	26	(	(	PUNCT
eurjchem-1252	81	27	0.24	0.24	NUM
eurjchem-1252	81	28	g	g	NOUN
eurjchem-1252	81	29	,	,	PUNCT
eurjchem-1252	81	30	3.66	3.66	NUM
eurjchem-1252	81	31	mmol	mmol	NOUN
eurjchem-1252	81	32	)	)	PUNCT
eurjchem-1252	81	33	in	in	ADP
eurjchem-1252	81	34	dimethylformamide	dimethylformamide	NOUN
eurjchem-1252	81	35	(	(	PUNCT
eurjchem-1252	81	36	10	10	NUM
eurjchem-1252	81	37	ml	ml	NOUN
eurjchem-1252	81	38	)	)	PUNCT
eurjchem-1252	81	39	was	be	AUX
eurjchem-1252	81	40	heated	heat	VERB
eurjchem-1252	81	41	at	at	ADP
eurjchem-1252	81	42	100	100	NUM
eurjchem-1252	81	43	°	°	ADP
eurjchem-1252	81	44	c	c	NOUN
eurjchem-1252	81	45	for	for	ADP
eurjchem-1252	81	46	3	3	NUM
eurjchem-1252	81	47	h.	h.	NOUN
eurjchem-1252	81	48	the	the	DET
eurjchem-1252	81	49	reaction	reaction	NOUN
eurjchem-1252	81	50	mixture	mixture	NOUN
eurjchem-1252	81	51	was	be	AUX
eurjchem-1252	81	52	cooled	cool	VERB
eurjchem-1252	81	53	,	,	PUNCT
eurjchem-1252	81	54	poured	pour	VERB
eurjchem-1252	81	55	into	into	ADP
eurjchem-1252	81	56	ice	ice	NOUN
eurjchem-1252	81	57	cold	cold	ADJ
eurjchem-1252	81	58	water	water	NOUN
eurjchem-1252	81	59	(	(	PUNCT
eurjchem-1252	81	60	100	100	NUM
eurjchem-1252	81	61	ml	ml	NOUN
eurjchem-1252	81	62	)	)	PUNCT
eurjchem-1252	81	63	.	.	PUNCT
eurjchem-1252	82	1	the	the	DET
eurjchem-1252	82	2	solid	solid	ADJ
eurjchem-1252	82	3	product	product	NOUN
eurjchem-1252	82	4	was	be	AUX
eurjchem-1252	82	5	filtered	filter	VERB
eurjchem-1252	82	6	off	off	ADP
eurjchem-1252	82	7	,	,	PUNCT
eurjchem-1252	82	8	washed	wash	VERB
eurjchem-1252	82	9	with	with	ADP
eurjchem-1252	82	10	water	water	NOUN
eurjchem-1252	82	11	,	,	PUNCT
eurjchem-1252	82	12	dried	dry	VERB
eurjchem-1252	82	13	,	,	PUNCT
eurjchem-1252	82	14	and	and	CCONJ
eurjchem-1252	82	15	recrystallized	recrystallize	VERB
eurjchem-1252	82	16	from	from	ADP
eurjchem-1252	82	17	ethanol	ethanol	NOUN
eurjchem-1252	82	18	to	to	PART
eurjchem-1252	82	19	give	give	VERB
eurjchem-1252	82	20	compound	compound	NOUN
eurjchem-1252	82	21	3c	3c	NUM
eurjchem-1252	82	22	(	(	PUNCT
eurjchem-1252	82	23	scheme	scheme	NOUN
eurjchem-1252	82	24	1	1	NUM
eurjchem-1252	82	25	)	)	PUNCT
eurjchem-1252	82	26	.	.	PUNCT
eurjchem-1252	83	1	color	color	NOUN
eurjchem-1252	83	2	:	:	PUNCT
eurjchem-1252	83	3	brown	brown	ADJ
eurjchem-1252	83	4	.	.	PUNCT
eurjchem-1252	84	1	yield	yield	NOUN
eurjchem-1252	84	2	:	:	PUNCT
eurjchem-1252	84	3	76.77	76.77	NUM
eurjchem-1252	84	4	%	%	NOUN
eurjchem-1252	84	5	.	.	PUNCT
eurjchem-1252	85	1	m.p	m.p	PROPN
eurjchem-1252	85	2	.	.	PROPN
eurjchem-1252	85	3	:	:	PUNCT
eurjchem-1252	86	1	190‐192	190‐192	NUM
eurjchem-1252	86	2	°	°	ADP
eurjchem-1252	86	3	c	c	X
eurjchem-1252	86	4	.	.	PUNCT
eurjchem-1252	87	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	87	2	(	(	PUNCT
eurjchem-1252	87	3	kbr	kbr	PROPN
eurjchem-1252	87	4	,	,	PUNCT
eurjchem-1252	87	5	ν	ν	PROPN
eurjchem-1252	87	6	,	,	PUNCT
eurjchem-1252	87	7	cm‐1	cm‐1	PROPN
eurjchem-1252	87	8	):	):	PUNCT
eurjchem-1252	87	9	3057	3057	NUM
eurjchem-1252	87	10	(	(	PUNCT
eurjchem-1252	87	11	ch	ch	NOUN
eurjchem-1252	87	12	,	,	PUNCT
eurjchem-1252	87	13	arom	arom	NOUN
eurjchem-1252	87	14	.	.	PUNCT
eurjchem-1252	87	15	)	)	PUNCT
eurjchem-1252	87	16	,	,	PUNCT
eurjchem-1252	87	17	2209	2209	NUM
eurjchem-1252	87	18	(	(	PUNCT
eurjchem-1252	87	19	n3	n3	NOUN
eurjchem-1252	87	20	)	)	PUNCT
eurjchem-1252	87	21	,	,	PUNCT
eurjchem-1252	87	22	1652	1652	NUM
eurjchem-1252	87	23	(	(	PUNCT
eurjchem-1252	87	24	c	c	NOUN
eurjchem-1252	87	25	=	=	NOUN
eurjchem-1252	87	26	o	o	NOUN
eurjchem-1252	87	27	)	)	PUNCT
eurjchem-1252	87	28	,	,	PUNCT
eurjchem-1252	87	29	1612	1612	NUM
eurjchem-1252	87	30	(	(	PUNCT
eurjchem-1252	87	31	c	c	NOUN
eurjchem-1252	87	32	=	=	SYM
eurjchem-1252	87	33	n	n	NUM
eurjchem-1252	87	34	)	)	PUNCT
eurjchem-1252	87	35	.	.	PUNCT
eurjchem-1252	88	1	1h	1h	NUM
eurjchem-1252	88	2	nmr	nmr	NOUN
eurjchem-1252	88	3	(	(	PUNCT
eurjchem-1252	88	4	300	300	NUM
eurjchem-1252	88	5	mhz	mhz	NOUN
eurjchem-1252	88	6	,	,	PUNCT
eurjchem-1252	88	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1252	88	8	,	,	PUNCT
eurjchem-1252	88	9	δ	δ	PROPN
eurjchem-1252	88	10	,	,	PUNCT
eurjchem-1252	88	11	ppm	ppm	NUM
eurjchem-1252	88	12	):	):	PUNCT
eurjchem-1252	88	13	5.88	5.88	NUM
eurjchem-1252	88	14	(	(	PUNCT
eurjchem-1252	88	15	s	s	PROPN
eurjchem-1252	88	16	,	,	PUNCT
eurjchem-1252	88	17	1h	1h	NUM
eurjchem-1252	88	18	,	,	PUNCT
eurjchem-1252	88	19	ch	ch	NOUN
eurjchem-1252	88	20	,	,	PUNCT
eurjchem-1252	88	21	pyrimidine	pyrimidine	NOUN
eurjchem-1252	88	22	ring	ring	NOUN
eurjchem-1252	88	23	)	)	PUNCT
eurjchem-1252	88	24	,	,	PUNCT
eurjchem-1252	88	25	6.89‐	6.89‐	NUM
eurjchem-1252	88	26	7.37	7.37	NUM
eurjchem-1252	88	27	(	(	PUNCT
eurjchem-1252	88	28	m	m	PROPN
eurjchem-1252	88	29	,	,	PUNCT
eurjchem-1252	88	30	15h	15h	NUM
eurjchem-1252	88	31	,	,	PUNCT
eurjchem-1252	88	32	3ph	3ph	NOUN
eurjchem-1252	88	33	)	)	PUNCT
eurjchem-1252	88	34	.	.	PUNCT
eurjchem-1252	89	1	ms	ms	NOUN
eurjchem-1252	89	2	(	(	PUNCT
eurjchem-1252	89	3	ei	ei	PROPN
eurjchem-1252	89	4	,	,	PUNCT
eurjchem-1252	89	5	m	m	PROPN
eurjchem-1252	89	6	/	/	SYM
eurjchem-1252	89	7	z	z	PROPN
eurjchem-1252	89	8	(	(	PUNCT
eurjchem-1252	89	9	%	%	NOUN
eurjchem-1252	89	10	)	)	PUNCT
eurjchem-1252	89	11	):	):	PUNCT
eurjchem-1252	89	12	416	416	NUM
eurjchem-1252	89	13	(	(	PUNCT
eurjchem-1252	89	14	m+	m+	NUM
eurjchem-1252	89	15	,	,	PUNCT
eurjchem-1252	89	16	3.20	3.20	NUM
eurjchem-1252	89	17	)	)	PUNCT
eurjchem-1252	89	18	,	,	PUNCT
eurjchem-1252	89	19	388	388	NUM
eurjchem-1252	89	20	(	(	PUNCT
eurjchem-1252	89	21	33.45	33.45	NUM
eurjchem-1252	89	22	)	)	PUNCT
eurjchem-1252	89	23	,	,	PUNCT
eurjchem-1252	89	24	374	374	NUM
eurjchem-1252	89	25	(	(	PUNCT
eurjchem-1252	89	26	5.81	5.81	NUM
eurjchem-1252	89	27	)	)	PUNCT
eurjchem-1252	89	28	,	,	PUNCT
eurjchem-1252	89	29	322	322	NUM
eurjchem-1252	89	30	(	(	PUNCT
eurjchem-1252	89	31	100	100	NUM
eurjchem-1252	89	32	)	)	PUNCT
eurjchem-1252	89	33	,	,	PUNCT
eurjchem-1252	89	34	237	237	NUM
eurjchem-1252	89	35	(	(	PUNCT
eurjchem-1252	89	36	7.83	7.83	NUM
eurjchem-1252	89	37	)	)	PUNCT
eurjchem-1252	89	38	,	,	PUNCT
eurjchem-1252	89	39	178	178	NUM
eurjchem-1252	89	40	(	(	PUNCT
eurjchem-1252	89	41	9.25	9.25	NUM
eurjchem-1252	89	42	)	)	PUNCT
eurjchem-1252	89	43	,	,	PUNCT
eurjchem-1252	89	44	77	77	NUM
eurjchem-1252	89	45	(	(	PUNCT
eurjchem-1252	89	46	17.08	17.08	NUM
eurjchem-1252	89	47	)	)	PUNCT
eurjchem-1252	89	48	.	.	PUNCT
eurjchem-1252	90	1	anal	anal	PROPN
eurjchem-1252	90	2	.	.	PUNCT
eurjchem-1252	90	3	calcd	calcd	NOUN
eurjchem-1252	90	4	.	.	PUNCT
eurjchem-1252	91	1	for	for	ADP
eurjchem-1252	91	2	c25h16n6o	c25h16n6o	NOUN
eurjchem-1252	91	3	:	:	PUNCT
eurjchem-1252	91	4	c	c	X
eurjchem-1252	91	5	,	,	PUNCT
eurjchem-1252	91	6	72.10	72.10	NUM
eurjchem-1252	91	7	;	;	PUNCT
eurjchem-1252	91	8	h	h	NOUN
eurjchem-1252	91	9	,	,	PUNCT
eurjchem-1252	91	10	3.87	3.87	NUM
eurjchem-1252	91	11	;	;	PUNCT
eurjchem-1252	91	12	n	n	CCONJ
eurjchem-1252	91	13	,	,	PUNCT
eurjchem-1252	91	14	20.18	20.18	NUM
eurjchem-1252	91	15	.	.	PUNCT
eurjchem-1252	91	16	found	find	VERB
eurjchem-1252	91	17	:	:	PUNCT
eurjchem-1252	92	1	c	c	X
eurjchem-1252	92	2	,	,	PUNCT
eurjchem-1252	92	3	72.48	72.48	NUM
eurjchem-1252	92	4	;	;	PUNCT
eurjchem-1252	92	5	h	h	NOUN
eurjchem-1252	92	6	,	,	PUNCT
eurjchem-1252	92	7	3.99	3.99	NUM
eurjchem-1252	92	8	;	;	PUNCT
eurjchem-1252	92	9	n	n	CCONJ
eurjchem-1252	92	10	,	,	PUNCT
eurjchem-1252	92	11	20.01	20.01	NUM
eurjchem-1252	92	12	%	%	NOUN
eurjchem-1252	92	13	.	.	PUNCT
eurjchem-1252	93	1	2.2.6	2.2.6	X
eurjchem-1252	93	2	.	.	PUNCT
eurjchem-1252	94	1	synthesis	synthesis	NOUN
eurjchem-1252	94	2	of	of	ADP
eurjchem-1252	94	3	2‐hydrazinyl‐7,8,9‐triphenyl‐4h‐	2‐hydrazinyl‐7,8,9‐triphenyl‐4h‐	NUM
eurjchem-1252	94	4	pyrimido[1,2‐b]pyridazin‐4‐one	pyrimido[1,2‐b]pyridazin‐4‐one	NOUN
eurjchem-1252	94	5	(	(	PUNCT
eurjchem-1252	94	6	3d	3d	NOUN
eurjchem-1252	94	7	)	)	PUNCT
eurjchem-1252	94	8	a	a	DET
eurjchem-1252	94	9	solution	solution	NOUN
eurjchem-1252	94	10	of	of	ADP
eurjchem-1252	94	11	compound	compound	NOUN
eurjchem-1252	94	12	2	2	NUM
eurjchem-1252	94	13	(	(	PUNCT
eurjchem-1252	94	14	0.5	0.5	NUM
eurjchem-1252	94	15	g	g	NOUN
eurjchem-1252	94	16	,	,	PUNCT
eurjchem-1252	94	17	1.22	1.22	NUM
eurjchem-1252	94	18	mmol	mmol	NOUN
eurjchem-1252	94	19	)	)	PUNCT
eurjchem-1252	94	20	,	,	PUNCT
eurjchem-1252	94	21	and	and	CCONJ
eurjchem-1252	94	22	hydrazine	hydrazine	NOUN
eurjchem-1252	94	23	hydrate	hydrate	NOUN
eurjchem-1252	94	24	(	(	PUNCT
eurjchem-1252	94	25	0.1	0.1	NUM
eurjchem-1252	94	26	ml	ml	NOUN
eurjchem-1252	94	27	,	,	PUNCT
eurjchem-1252	94	28	1.22	1.22	NUM
eurjchem-1252	94	29	mmol	mmol	NOUN
eurjchem-1252	94	30	)	)	PUNCT
eurjchem-1252	94	31	in	in	ADP
eurjchem-1252	94	32	ethanol	ethanol	NOUN
eurjchem-1252	94	33	(	(	PUNCT
eurjchem-1252	94	34	10	10	NUM
eurjchem-1252	94	35	ml	ml	NOUN
eurjchem-1252	94	36	)	)	PUNCT
eurjchem-1252	94	37	was	be	AUX
eurjchem-1252	94	38	heated	heat	VERB
eurjchem-1252	94	39	under	under	ADP
eurjchem-1252	94	40	reflux	reflux	NOUN
eurjchem-1252	94	41	for	for	ADP
eurjchem-1252	94	42	3	3	NUM
eurjchem-1252	94	43	h.	h.	NOUN
eurjchem-1252	94	44	206	206	NUM
eurjchem-1252	94	45	deeb	deeb	PROPN
eurjchem-1252	94	46	et	et	PROPN
eurjchem-1252	94	47	al	al	PROPN
eurjchem-1252	94	48	.	.	PUNCT
eurjchem-1252	94	49	/	/	SYM
eurjchem-1252	94	50	european	european	PROPN
eurjchem-1252	94	51	journal	journal	PROPN
eurjchem-1252	94	52	of	of	ADP
eurjchem-1252	94	53	chemistry	chemistry	NOUN
eurjchem-1252	94	54	6	6	NUM
eurjchem-1252	94	55	(	(	PUNCT
eurjchem-1252	94	56	2	2	NUM
eurjchem-1252	94	57	)	)	PUNCT
eurjchem-1252	94	58	(	(	PUNCT
eurjchem-1252	94	59	2015	2015	NUM
eurjchem-1252	94	60	)	)	PUNCT
eurjchem-1252	94	61	204‐210	204‐210	NOUN
eurjchem-1252	94	62	n	n	CCONJ
eurjchem-1252	94	63	n	n	CCONJ
eurjchem-1252	94	64	n	n	NOUN
eurjchem-1252	94	65	o	o	NOUN
eurjchem-1252	94	66	o	o	X
eurjchem-1252	94	67	ph	ph	ADJ
eurjchem-1252	94	68	ph	ph	ADJ
eurjchem-1252	94	69	ph	ph	NOUN
eurjchem-1252	94	70	no2	no2	PROPN
eurjchem-1252	94	71	10	10	NUM
eurjchem-1252	94	72	r.t	r.t	PROPN
eurjchem-1252	94	73	.	.	PROPN
eurjchem-1252	94	74	,	,	PUNCT
eurjchem-1252	94	75	2	2	NUM
eurjchem-1252	94	76	h	h	NOUN
eurjchem-1252	94	77	n	n	CCONJ
eurjchem-1252	94	78	n	n	CCONJ
eurjchem-1252	94	79	n	n	ADV
eurjchem-1252	94	80	o	o	X
eurjchem-1252	94	81	ph	ph	ADJ
eurjchem-1252	94	82	ph	ph	ADJ
eurjchem-1252	94	83	ph	ph	NOUN
eurjchem-1252	94	84	cl	cl	NOUN
eurjchem-1252	94	85	no2	no2	NOUN
eurjchem-1252	94	86	11	11	NUM
eurjchem-1252	94	87	n	n	CCONJ
eurjchem-1252	94	88	n	n	CCONJ
eurjchem-1252	94	89	n	n	NOUN
eurjchem-1252	94	90	o	o	NOUN
eurjchem-1252	94	91	o	o	X
eurjchem-1252	94	92	ph	ph	ADJ
eurjchem-1252	94	93	ph	ph	ADJ
eurjchem-1252	94	94	ph	ph	NOUN
eurjchem-1252	94	95	nh2	nh2	NOUN
eurjchem-1252	94	96	9	9	NUM
eurjchem-1252	94	97	n	n	CCONJ
eurjchem-1252	94	98	n	n	CCONJ
eurjchem-1252	94	99	n	n	NOUN
eurjchem-1252	94	100	o	o	NOUN
eurjchem-1252	94	101	o	o	X
eurjchem-1252	94	102	ph	ph	ADJ
eurjchem-1252	94	103	ph	ph	ADJ
eurjchem-1252	94	104	ph	ph	NOUN
eurjchem-1252	94	105	cl	cl	NOUN
eurjchem-1252	94	106	cl	cl	NOUN
eurjchem-1252	94	107	6	6	NUM
eurjchem-1252	94	108	n	n	NOUN
eurjchem-1252	94	109	n	n	CCONJ
eurjchem-1252	94	110	n	n	NOUN
eurjchem-1252	94	111	o	o	NOUN
eurjchem-1252	94	112	o	o	X
eurjchem-1252	94	113	ph	ph	ADJ
eurjchem-1252	94	114	ph	ph	ADJ
eurjchem-1252	94	115	ph	ph	NOUN
eurjchem-1252	94	116	cl	cl	NOUN
eurjchem-1252	94	117	87	87	NUM
eurjchem-1252	94	118	n	n	CCONJ
eurjchem-1252	94	119	n	n	PRON
eurjchem-1252	94	120	ph	ph	ADJ
eurjchem-1252	94	121	ph	ph	NOUN
eurjchem-1252	94	122	ph	ph	NOUN
eurjchem-1252	94	123	n	n	NOUN
eurjchem-1252	94	124	o	o	NOUN
eurjchem-1252	94	125	cl	cl	NOUN
eurjchem-1252	94	126	n	n	CCONJ
eurjchem-1252	94	127	n	n	CCONJ
eurjchem-1252	94	128	n	n	ADV
eurjchem-1252	94	129	o	o	NOUN
eurjchem-1252	94	130	o	o	X
eurjchem-1252	95	1	ph	ph	NOUN
eurjchem-1252	95	2	ph	ph	NOUN
eurjchem-1252	95	3	ph	ph	NOUN
eurjchem-1252	95	4	br	br	NOUN
eurjchem-1252	95	5	br	br	NOUN
eurjchem-1252	95	6	5	5	NUM
eurjchem-1252	95	7	aq	aq	NOUN
eurjchem-1252	95	8	.	.	PROPN
eurjchem-1252	95	9	na2co3	na2co3	PROPN
eurjchem-1252	95	10	reflux	reflux	VERB
eurjchem-1252	95	11	6	6	NUM
eurjchem-1252	95	12	h	h	NOUN
eurjchem-1252	95	13	zn	zn	NOUN
eurjchem-1252	95	14	/	/	SYM
eurjchem-1252	95	15	acoh	acoh	ADJ
eurjchem-1252	95	16	,	,	PUNCT
eurjchem-1252	95	17	reflux	reflux	VERB
eurjchem-1252	95	18	1.5	1.5	NUM
eurjchem-1252	95	19	h	h	NOUN
eurjchem-1252	95	20	reflux	reflux	NOUN
eurjchem-1252	96	1	30	30	NUM
eurjchem-1252	96	2	min	min	NOUN
eurjchem-1252	96	3	.	.	PROPN
eurjchem-1252	96	4	acoh	acoh	PROPN
eurjchem-1252	96	5	/	/	SYM
eurjchem-1252	96	6	nano2	nano2	PROPN
eurjchem-1252	96	7	/	/	SYM
eurjchem-1252	96	8	hno3	hno3	PROPN
eurjchem-1252	96	9	70	70	NUM
eurjchem-1252	96	10	oc	oc	NOUN
eurjchem-1252	96	11	,	,	PUNCT
eurjchem-1252	96	12	stirring	stir	VERB
eurjchem-1252	96	13	for	for	ADP
eurjchem-1252	96	14	1	1	NUM
eurjchem-1252	96	15	h	h	NOUN
eurjchem-1252	96	16	zn	zn	PROPN
eurjchem-1252	96	17	/	/	SYM
eurjchem-1252	96	18	acoh	acoh	ADJ
eurjchem-1252	96	19	,	,	PUNCT
eurjchem-1252	96	20	reflux	reflux	NOUN
eurjchem-1252	96	21	3	3	NUM
eurjchem-1252	96	22	h	h	NOUN
eurjchem-1252	96	23	reflux	reflux	NOUN
eurjchem-1252	96	24	2	2	NUM
eurjchem-1252	96	25	h	h	NOUN
eurjchem-1252	96	26	sand	sand	NOUN
eurjchem-1252	96	27	bath	bath	NOUN
eurjchem-1252	96	28	,	,	PUNCT
eurjchem-1252	96	29	210	210	NUM
eurjchem-1252	96	30	oc	oc	NOUN
eurjchem-1252	96	31	for	for	ADP
eurjchem-1252	96	32	30	30	NUM
eurjchem-1252	96	33	min	min	NOUN
eurjchem-1252	96	34	br2	br2	PROPN
eurjchem-1252	96	35	,	,	PUNCT
eurjchem-1252	96	36	chcl3	chcl3	PROPN
eurjchem-1252	96	37	so2cl2	so2cl2	X
eurjchem-1252	96	38	pocl3	pocl3	X
eurjchem-1252	96	39	aconh4	aconh4	PROPN
eurjchem-1252	97	1	n	n	CCONJ
eurjchem-1252	97	2	n	n	CCONJ
eurjchem-1252	97	3	n	n	ADV
eurjchem-1252	97	4	o	o	NOUN
eurjchem-1252	97	5	o	o	X
eurjchem-1252	97	6	ph	ph	NOUN
eurjchem-1252	97	7	ph	ph	ADJ
eurjchem-1252	97	8	ph	ph	NOUN
eurjchem-1252	97	9	1	1	NUM
eurjchem-1252	97	10	scheme	scheme	NOUN
eurjchem-1252	97	11	2	2	NUM
eurjchem-1252	97	12	the	the	DET
eurjchem-1252	97	13	solvent	solvent	NOUN
eurjchem-1252	97	14	was	be	AUX
eurjchem-1252	97	15	evaporated	evaporate	VERB
eurjchem-1252	97	16	,	,	PUNCT
eurjchem-1252	97	17	and	and	CCONJ
eurjchem-1252	97	18	the	the	DET
eurjchem-1252	97	19	residue	residue	NOUN
eurjchem-1252	97	20	was	be	AUX
eurjchem-1252	97	21	triturated	triturate	VERB
eurjchem-1252	97	22	with	with	ADP
eurjchem-1252	97	23	cold	cold	ADJ
eurjchem-1252	97	24	water	water	NOUN
eurjchem-1252	97	25	.	.	PUNCT
eurjchem-1252	98	1	the	the	DET
eurjchem-1252	98	2	solid	solid	ADJ
eurjchem-1252	98	3	product	product	NOUN
eurjchem-1252	98	4	formed	form	VERB
eurjchem-1252	98	5	was	be	AUX
eurjchem-1252	98	6	filtered	filter	VERB
eurjchem-1252	98	7	off	off	ADP
eurjchem-1252	98	8	,	,	PUNCT
eurjchem-1252	98	9	washed	wash	VERB
eurjchem-1252	98	10	with	with	ADP
eurjchem-1252	98	11	water	water	NOUN
eurjchem-1252	98	12	,	,	PUNCT
eurjchem-1252	98	13	dried	dry	VERB
eurjchem-1252	98	14	,	,	PUNCT
eurjchem-1252	98	15	and	and	CCONJ
eurjchem-1252	98	16	recrystallized	recrystallize	VERB
eurjchem-1252	98	17	from	from	ADP
eurjchem-1252	98	18	ethanol	ethanol	NOUN
eurjchem-1252	98	19	to	to	PART
eurjchem-1252	98	20	give	give	VERB
eurjchem-1252	98	21	compound	compound	NOUN
eurjchem-1252	98	22	3d	3d	NOUN
eurjchem-1252	98	23	(	(	PUNCT
eurjchem-1252	98	24	scheme	scheme	NOUN
eurjchem-1252	98	25	1	1	NUM
eurjchem-1252	98	26	)	)	PUNCT
eurjchem-1252	98	27	.	.	PUNCT
eurjchem-1252	99	1	color	color	NOUN
eurjchem-1252	99	2	:	:	PUNCT
eurjchem-1252	99	3	brown	brown	ADJ
eurjchem-1252	99	4	.	.	PUNCT
eurjchem-1252	100	1	yield	yield	NOUN
eurjchem-1252	100	2	:	:	PUNCT
eurjchem-1252	100	3	68.69	68.69	NUM
eurjchem-1252	100	4	%	%	NOUN
eurjchem-1252	100	5	.	.	PUNCT
eurjchem-1252	101	1	m.p	m.p	PROPN
eurjchem-1252	101	2	.	.	PROPN
eurjchem-1252	101	3	:	:	PUNCT
eurjchem-1252	102	1	>	>	X
eurjchem-1252	102	2	300	300	NUM
eurjchem-1252	102	3	°	°	SYM
eurjchem-1252	102	4	c	c	NOUN
eurjchem-1252	102	5	.	.	PUNCT
eurjchem-1252	103	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	103	2	(	(	PUNCT
eurjchem-1252	103	3	kbr	kbr	PROPN
eurjchem-1252	103	4	,	,	PUNCT
eurjchem-1252	103	5	ν	ν	PROPN
eurjchem-1252	103	6	,	,	PUNCT
eurjchem-1252	103	7	cm‐1	cm‐1	PROPN
eurjchem-1252	103	8	):	):	PUNCT
eurjchem-1252	103	9	3313	3313	NUM
eurjchem-1252	103	10	,	,	PUNCT
eurjchem-1252	103	11	3204	3204	NUM
eurjchem-1252	103	12	(	(	PUNCT
eurjchem-1252	103	13	nh	nh	PROPN
eurjchem-1252	103	14	,	,	PUNCT
eurjchem-1252	103	15	nh2	nh2	PROPN
eurjchem-1252	103	16	)	)	PUNCT
eurjchem-1252	103	17	,	,	PUNCT
eurjchem-1252	103	18	3058	3058	NUM
eurjchem-1252	103	19	(	(	PUNCT
eurjchem-1252	103	20	c‒h	c‒h	PROPN
eurjchem-1252	103	21	,	,	PUNCT
eurjchem-1252	103	22	arom	arom	NOUN
eurjchem-1252	103	23	.	.	PUNCT
eurjchem-1252	103	24	)	)	PUNCT
eurjchem-1252	103	25	,	,	PUNCT
eurjchem-1252	103	26	1691	1691	NUM
eurjchem-1252	103	27	(	(	PUNCT
eurjchem-1252	103	28	c	c	NOUN
eurjchem-1252	103	29	=	=	NOUN
eurjchem-1252	103	30	o	o	NOUN
eurjchem-1252	103	31	)	)	PUNCT
eurjchem-1252	103	32	.	.	PUNCT
eurjchem-1252	104	1	ms	ms	NOUN
eurjchem-1252	104	2	(	(	PUNCT
eurjchem-1252	104	3	ei	ei	PROPN
eurjchem-1252	104	4	,	,	PUNCT
eurjchem-1252	104	5	m	m	PROPN
eurjchem-1252	104	6	/	/	SYM
eurjchem-1252	104	7	z	z	PROPN
eurjchem-1252	104	8	(	(	PUNCT
eurjchem-1252	104	9	%	%	NOUN
eurjchem-1252	104	10	)	)	PUNCT
eurjchem-1252	104	11	):	):	PUNCT
eurjchem-1252	104	12	405	405	NUM
eurjchem-1252	104	13	(	(	PUNCT
eurjchem-1252	104	14	m+	m+	NUM
eurjchem-1252	104	15	,	,	PUNCT
eurjchem-1252	104	16	7.26	7.26	NUM
eurjchem-1252	104	17	)	)	PUNCT
eurjchem-1252	104	18	,	,	PUNCT
eurjchem-1252	104	19	388	388	NUM
eurjchem-1252	104	20	(	(	PUNCT
eurjchem-1252	104	21	6.15	6.15	NUM
eurjchem-1252	104	22	)	)	PUNCT
eurjchem-1252	104	23	,	,	PUNCT
eurjchem-1252	104	24	322	322	NUM
eurjchem-1252	104	25	(	(	PUNCT
eurjchem-1252	104	26	100	100	NUM
eurjchem-1252	104	27	)	)	PUNCT
eurjchem-1252	104	28	,	,	PUNCT
eurjchem-1252	104	29	306	306	NUM
eurjchem-1252	104	30	(	(	PUNCT
eurjchem-1252	104	31	5.49	5.49	NUM
eurjchem-1252	104	32	)	)	PUNCT
eurjchem-1252	104	33	,	,	PUNCT
eurjchem-1252	104	34	251	251	NUM
eurjchem-1252	104	35	(	(	PUNCT
eurjchem-1252	104	36	4.10	4.10	NUM
eurjchem-1252	104	37	)	)	PUNCT
eurjchem-1252	104	38	,	,	PUNCT
eurjchem-1252	104	39	178	178	NUM
eurjchem-1252	104	40	(	(	PUNCT
eurjchem-1252	104	41	10.99	10.99	NUM
eurjchem-1252	104	42	)	)	PUNCT
eurjchem-1252	104	43	,	,	PUNCT
eurjchem-1252	104	44	98	98	NUM
eurjchem-1252	104	45	(	(	PUNCT
eurjchem-1252	104	46	3.26	3.26	NUM
eurjchem-1252	104	47	)	)	PUNCT
eurjchem-1252	104	48	,	,	PUNCT
eurjchem-1252	104	49	77	77	NUM
eurjchem-1252	104	50	(	(	PUNCT
eurjchem-1252	104	51	17.97	17.97	NUM
eurjchem-1252	104	52	)	)	PUNCT
eurjchem-1252	104	53	.	.	PUNCT
eurjchem-1252	105	1	anal	anal	PROPN
eurjchem-1252	105	2	.	.	PUNCT
eurjchem-1252	105	3	calcd	calcd	NOUN
eurjchem-1252	105	4	.	.	PUNCT
eurjchem-1252	106	1	for	for	ADP
eurjchem-1252	106	2	c25h19n5o	c25h19n5o	NOUN
eurjchem-1252	106	3	:	:	PUNCT
eurjchem-1252	106	4	c	c	X
eurjchem-1252	106	5	,	,	PUNCT
eurjchem-1252	106	6	74.06	74.06	NUM
eurjchem-1252	106	7	;	;	PUNCT
eurjchem-1252	106	8	h	h	NOUN
eurjchem-1252	106	9	,	,	PUNCT
eurjchem-1252	106	10	4.72	4.72	NUM
eurjchem-1252	106	11	;	;	PUNCT
eurjchem-1252	106	12	n	n	CCONJ
eurjchem-1252	106	13	,	,	PUNCT
eurjchem-1252	106	14	17.27	17.27	NUM
eurjchem-1252	106	15	.	.	PUNCT
eurjchem-1252	106	16	found	find	VERB
eurjchem-1252	106	17	:	:	PUNCT
eurjchem-1252	107	1	c	c	X
eurjchem-1252	107	2	,	,	PUNCT
eurjchem-1252	107	3	74.38	74.38	NUM
eurjchem-1252	107	4	;	;	PUNCT
eurjchem-1252	107	5	h	h	X
eurjchem-1252	107	6	,	,	PUNCT
eurjchem-1252	107	7	4.83	4.83	NUM
eurjchem-1252	107	8	;	;	PUNCT
eurjchem-1252	107	9	n	n	CCONJ
eurjchem-1252	107	10	,	,	PUNCT
eurjchem-1252	107	11	17.54	17.54	NUM
eurjchem-1252	107	12	%	%	NOUN
eurjchem-1252	107	13	.	.	PUNCT
eurjchem-1252	108	1	2.2.7	2.2.7	X
eurjchem-1252	108	2	.	.	PUNCT
eurjchem-1252	109	1	synthesis	synthesis	NOUN
eurjchem-1252	109	2	of	of	ADP
eurjchem-1252	109	3	7,8,9‐triphenyl‐2‐thioxo‐2h‐pyrimido	7,8,9‐triphenyl‐2‐thioxo‐2h‐pyrimido	NOUN
eurjchem-1252	110	1	[	[	X
eurjchem-1252	110	2	1,2‐b]pyridazin‐4(3h)‐one	1,2‐b]pyridazin‐4(3h)‐one	NUM
eurjchem-1252	110	3	(	(	PUNCT
eurjchem-1252	110	4	4	4	NUM
eurjchem-1252	110	5	)	)	PUNCT
eurjchem-1252	110	6	a	a	DET
eurjchem-1252	110	7	solution	solution	NOUN
eurjchem-1252	110	8	of	of	ADP
eurjchem-1252	110	9	compound	compound	NOUN
eurjchem-1252	110	10	2	2	NUM
eurjchem-1252	110	11	(	(	PUNCT
eurjchem-1252	110	12	0.5	0.5	NUM
eurjchem-1252	110	13	g	g	NOUN
eurjchem-1252	110	14	,	,	PUNCT
eurjchem-1252	110	15	1.22	1.22	NUM
eurjchem-1252	110	16	mmol	mmol	NOUN
eurjchem-1252	110	17	)	)	PUNCT
eurjchem-1252	110	18	,	,	PUNCT
eurjchem-1252	110	19	and	and	CCONJ
eurjchem-1252	110	20	thiourea	thiourea	NOUN
eurjchem-1252	110	21	(	(	PUNCT
eurjchem-1252	110	22	0.5	0.5	NUM
eurjchem-1252	110	23	g	g	NOUN
eurjchem-1252	110	24	)	)	PUNCT
eurjchem-1252	110	25	in	in	ADP
eurjchem-1252	110	26	ethanol	ethanol	NOUN
eurjchem-1252	110	27	(	(	PUNCT
eurjchem-1252	110	28	10	10	NUM
eurjchem-1252	110	29	ml	ml	NOUN
eurjchem-1252	110	30	)	)	PUNCT
eurjchem-1252	110	31	was	be	AUX
eurjchem-1252	110	32	heated	heat	VERB
eurjchem-1252	110	33	under	under	ADP
eurjchem-1252	110	34	reflux	reflux	NOUN
eurjchem-1252	110	35	for	for	ADP
eurjchem-1252	110	36	2	2	NUM
eurjchem-1252	110	37	h.	h.	NOUN
eurjchem-1252	110	38	the	the	DET
eurjchem-1252	110	39	solvent	solvent	NOUN
eurjchem-1252	110	40	was	be	AUX
eurjchem-1252	110	41	evaporated	evaporate	VERB
eurjchem-1252	110	42	,	,	PUNCT
eurjchem-1252	110	43	and	and	CCONJ
eurjchem-1252	110	44	the	the	DET
eurjchem-1252	110	45	residue	residue	NOUN
eurjchem-1252	110	46	was	be	AUX
eurjchem-1252	110	47	dissolved	dissolve	VERB
eurjchem-1252	110	48	in	in	ADP
eurjchem-1252	110	49	sodium	sodium	NOUN
eurjchem-1252	110	50	hydroxide	hydroxide	NOUN
eurjchem-1252	110	51	(	(	PUNCT
eurjchem-1252	110	52	10	10	NUM
eurjchem-1252	110	53	%	%	NOUN
eurjchem-1252	110	54	)	)	PUNCT
eurjchem-1252	110	55	.	.	PUNCT
eurjchem-1252	111	1	the	the	DET
eurjchem-1252	111	2	reaction	reaction	NOUN
eurjchem-1252	111	3	mixture	mixture	NOUN
eurjchem-1252	111	4	was	be	AUX
eurjchem-1252	111	5	heated	heat	VERB
eurjchem-1252	111	6	under	under	ADP
eurjchem-1252	111	7	reflux	reflux	NOUN
eurjchem-1252	111	8	for	for	ADP
eurjchem-1252	111	9	30	30	NUM
eurjchem-1252	111	10	min	min	NOUN
eurjchem-1252	111	11	.	.	PROPN
eurjchem-1252	111	12	,	,	PUNCT
eurjchem-1252	111	13	and	and	CCONJ
eurjchem-1252	111	14	filtered	filter	VERB
eurjchem-1252	111	15	on	on	ADP
eurjchem-1252	111	16	hot	hot	ADJ
eurjchem-1252	111	17	.	.	PUNCT
eurjchem-1252	112	1	the	the	DET
eurjchem-1252	112	2	filtrate	filtrate	NOUN
eurjchem-1252	112	3	was	be	AUX
eurjchem-1252	112	4	cooled	cool	VERB
eurjchem-1252	112	5	,	,	PUNCT
eurjchem-1252	112	6	neutralized	neutralize	VERB
eurjchem-1252	112	7	with	with	ADP
eurjchem-1252	112	8	hydrochloric	hydrochloric	ADJ
eurjchem-1252	112	9	acid	acid	NOUN
eurjchem-1252	112	10	;	;	PUNCT
eurjchem-1252	112	11	the	the	DET
eurjchem-1252	112	12	formed	form	VERB
eurjchem-1252	112	13	precipitate	precipitate	NOUN
eurjchem-1252	112	14	was	be	AUX
eurjchem-1252	112	15	filtered	filter	VERB
eurjchem-1252	112	16	off	off	ADP
eurjchem-1252	112	17	,	,	PUNCT
eurjchem-1252	112	18	washed	wash	VERB
eurjchem-1252	112	19	with	with	ADP
eurjchem-1252	112	20	water	water	NOUN
eurjchem-1252	112	21	,	,	PUNCT
eurjchem-1252	112	22	dried	dry	VERB
eurjchem-1252	112	23	,	,	PUNCT
eurjchem-1252	112	24	and	and	CCONJ
eurjchem-1252	112	25	recrystallized	recrystallize	VERB
eurjchem-1252	112	26	from	from	ADP
eurjchem-1252	112	27	ethanol	ethanol	NOUN
eurjchem-1252	112	28	to	to	PART
eurjchem-1252	112	29	give	give	VERB
eurjchem-1252	112	30	compound	compound	NOUN
eurjchem-1252	112	31	4	4	NUM
eurjchem-1252	112	32	(	(	PUNCT
eurjchem-1252	112	33	scheme	scheme	NOUN
eurjchem-1252	112	34	1	1	NUM
eurjchem-1252	112	35	)	)	PUNCT
eurjchem-1252	112	36	.	.	PUNCT
eurjchem-1252	113	1	color	color	NOUN
eurjchem-1252	113	2	:	:	PUNCT
eurjchem-1252	113	3	brown	brown	ADJ
eurjchem-1252	113	4	.	.	PUNCT
eurjchem-1252	114	1	yield	yield	NOUN
eurjchem-1252	114	2	:	:	PUNCT
eurjchem-1252	114	3	68.4	68.4	NUM
eurjchem-1252	114	4	%	%	NOUN
eurjchem-1252	114	5	.	.	PUNCT
eurjchem-1252	115	1	m.p	m.p	PROPN
eurjchem-1252	115	2	.	.	PROPN
eurjchem-1252	115	3	:	:	PUNCT
eurjchem-1252	116	1	212‐213	212‐213	NUM
eurjchem-1252	116	2	°	°	SYM
eurjchem-1252	116	3	c	c	X
eurjchem-1252	116	4	.	.	PUNCT
eurjchem-1252	117	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	117	2	(	(	PUNCT
eurjchem-1252	117	3	kbr	kbr	PROPN
eurjchem-1252	117	4	,	,	PUNCT
eurjchem-1252	117	5	ν	ν	PROPN
eurjchem-1252	117	6	,	,	PUNCT
eurjchem-1252	117	7	cm‐1	cm‐1	PROPN
eurjchem-1252	117	8	):	):	PUNCT
eurjchem-1252	117	9	3057	3057	NUM
eurjchem-1252	117	10	(	(	PUNCT
eurjchem-1252	117	11	ch	ch	NOUN
eurjchem-1252	117	12	,	,	PUNCT
eurjchem-1252	117	13	arom	arom	NOUN
eurjchem-1252	117	14	.	.	PUNCT
eurjchem-1252	117	15	)	)	PUNCT
eurjchem-1252	117	16	,	,	PUNCT
eurjchem-1252	117	17	2968	2968	NUM
eurjchem-1252	117	18	,	,	PUNCT
eurjchem-1252	117	19	2926	2926	NUM
eurjchem-1252	117	20	(	(	PUNCT
eurjchem-1252	117	21	ch	ch	NOUN
eurjchem-1252	117	22	,	,	PUNCT
eurjchem-1252	117	23	aliph	aliph	NOUN
eurjchem-1252	117	24	.	.	PUNCT
eurjchem-1252	117	25	)	)	PUNCT
eurjchem-1252	117	26	,	,	PUNCT
eurjchem-1252	117	27	1705	1705	NUM
eurjchem-1252	117	28	(	(	PUNCT
eurjchem-1252	117	29	c	c	NOUN
eurjchem-1252	117	30	=	=	NOUN
eurjchem-1252	117	31	o	o	NOUN
eurjchem-1252	117	32	)	)	PUNCT
eurjchem-1252	117	33	,	,	PUNCT
eurjchem-1252	117	34	1638	1638	NUM
eurjchem-1252	117	35	(	(	PUNCT
eurjchem-1252	117	36	c	c	NOUN
eurjchem-1252	117	37	=	=	SYM
eurjchem-1252	117	38	n	n	NUM
eurjchem-1252	117	39	)	)	PUNCT
eurjchem-1252	117	40	,	,	PUNCT
eurjchem-1252	117	41	1236	1236	NUM
eurjchem-1252	117	42	(	(	PUNCT
eurjchem-1252	117	43	c	c	NOUN
eurjchem-1252	117	44	=	=	SYM
eurjchem-1252	117	45	s	s	NOUN
eurjchem-1252	117	46	)	)	PUNCT
eurjchem-1252	117	47	.	.	PUNCT
eurjchem-1252	118	1	ms	ms	NOUN
eurjchem-1252	118	2	(	(	PUNCT
eurjchem-1252	118	3	ei	ei	PROPN
eurjchem-1252	118	4	,	,	PUNCT
eurjchem-1252	118	5	m	m	PROPN
eurjchem-1252	118	6	/	/	SYM
eurjchem-1252	118	7	z	z	PROPN
eurjchem-1252	118	8	(	(	PUNCT
eurjchem-1252	118	9	%	%	NOUN
eurjchem-1252	118	10	)	)	PUNCT
eurjchem-1252	118	11	):	):	PUNCT
eurjchem-1252	118	12	407	407	NUM
eurjchem-1252	118	13	(	(	PUNCT
eurjchem-1252	118	14	m+	m+	NUM
eurjchem-1252	118	15	,	,	PUNCT
eurjchem-1252	118	16	44.59	44.59	NUM
eurjchem-1252	118	17	)	)	PUNCT
eurjchem-1252	118	18	,	,	PUNCT
eurjchem-1252	118	19	377	377	NUM
eurjchem-1252	118	20	(	(	PUNCT
eurjchem-1252	118	21	36.31	36.31	NUM
eurjchem-1252	118	22	)	)	PUNCT
eurjchem-1252	118	23	,	,	PUNCT
eurjchem-1252	118	24	349	349	NUM
eurjchem-1252	118	25	(	(	PUNCT
eurjchem-1252	118	26	39.49	39.49	NUM
eurjchem-1252	118	27	)	)	PUNCT
eurjchem-1252	118	28	,	,	PUNCT
eurjchem-1252	118	29	336	336	NUM
eurjchem-1252	118	30	(	(	PUNCT
eurjchem-1252	118	31	51.59	51.59	NUM
eurjchem-1252	118	32	)	)	PUNCT
eurjchem-1252	118	33	,	,	PUNCT
eurjchem-1252	118	34	320	320	NUM
eurjchem-1252	118	35	(	(	PUNCT
eurjchem-1252	118	36	33.12	33.12	NUM
eurjchem-1252	118	37	)	)	PUNCT
eurjchem-1252	118	38	,	,	PUNCT
eurjchem-1252	118	39	307	307	NUM
eurjchem-1252	118	40	(	(	PUNCT
eurjchem-1252	118	41	38.22	38.22	NUM
eurjchem-1252	118	42	)	)	PUNCT
eurjchem-1252	118	43	,	,	PUNCT
eurjchem-1252	118	44	268	268	NUM
eurjchem-1252	118	45	(	(	PUNCT
eurjchem-1252	118	46	42.04	42.04	NUM
eurjchem-1252	118	47	)	)	PUNCT
eurjchem-1252	118	48	,	,	PUNCT
eurjchem-1252	118	49	229	229	NUM
eurjchem-1252	118	50	(	(	PUNCT
eurjchem-1252	118	51	35.03	35.03	NUM
eurjchem-1252	118	52	)	)	PUNCT
eurjchem-1252	118	53	,	,	PUNCT
eurjchem-1252	118	54	178	178	NUM
eurjchem-1252	118	55	(	(	PUNCT
eurjchem-1252	118	56	35.03	35.03	NUM
eurjchem-1252	118	57	)	)	PUNCT
eurjchem-1252	118	58	,	,	PUNCT
eurjchem-1252	118	59	139	139	NUM
eurjchem-1252	118	60	(	(	PUNCT
eurjchem-1252	118	61	44.59	44.59	NUM
eurjchem-1252	118	62	)	)	PUNCT
eurjchem-1252	118	63	,	,	PUNCT
eurjchem-1252	118	64	100	100	NUM
eurjchem-1252	118	65	(	(	PUNCT
eurjchem-1252	118	66	7.01	7.01	NUM
eurjchem-1252	118	67	)	)	PUNCT
eurjchem-1252	118	68	,	,	PUNCT
eurjchem-1252	118	69	86	86	NUM
eurjchem-1252	118	70	(	(	PUNCT
eurjchem-1252	118	71	45.22	45.22	NUM
eurjchem-1252	118	72	)	)	PUNCT
eurjchem-1252	118	73	,	,	PUNCT
eurjchem-1252	118	74	64	64	NUM
eurjchem-1252	118	75	(	(	PUNCT
eurjchem-1252	118	76	100	100	NUM
eurjchem-1252	118	77	)	)	PUNCT
eurjchem-1252	118	78	.	.	PUNCT
eurjchem-1252	119	1	anal	anal	PROPN
eurjchem-1252	119	2	.	.	PUNCT
eurjchem-1252	119	3	calcd	calcd	NOUN
eurjchem-1252	119	4	.	.	PUNCT
eurjchem-1252	120	1	for	for	ADP
eurjchem-1252	120	2	c25h17n3os	c25h17n3os	NOUN
eurjchem-1252	120	3	:	:	PUNCT
eurjchem-1252	120	4	c	c	X
eurjchem-1252	120	5	,	,	PUNCT
eurjchem-1252	120	6	73.69	73.69	NUM
eurjchem-1252	120	7	;	;	PUNCT
eurjchem-1252	120	8	h	h	NOUN
eurjchem-1252	120	9	,	,	PUNCT
eurjchem-1252	120	10	4.21	4.21	NUM
eurjchem-1252	120	11	;	;	PUNCT
eurjchem-1252	120	12	n	n	CCONJ
eurjchem-1252	120	13	,	,	PUNCT
eurjchem-1252	120	14	10.31	10.31	NUM
eurjchem-1252	120	15	.	.	PUNCT
eurjchem-1252	120	16	found	find	VERB
eurjchem-1252	120	17	:	:	PUNCT
eurjchem-1252	121	1	c	c	X
eurjchem-1252	121	2	,	,	PUNCT
eurjchem-1252	121	3	73.98	73.98	NUM
eurjchem-1252	121	4	;	;	PUNCT
eurjchem-1252	121	5	h	h	NOUN
eurjchem-1252	121	6	,	,	PUNCT
eurjchem-1252	121	7	4.06	4.06	NUM
eurjchem-1252	121	8	;	;	PUNCT
eurjchem-1252	121	9	n	n	CCONJ
eurjchem-1252	121	10	,	,	PUNCT
eurjchem-1252	121	11	10.53	10.53	NUM
eurjchem-1252	121	12	%	%	NOUN
eurjchem-1252	121	13	.	.	PUNCT
eurjchem-1252	122	1	2.2.8	2.2.8	X
eurjchem-1252	122	2	.	.	PUNCT
eurjchem-1252	123	1	synthesis	synthesis	NOUN
eurjchem-1252	123	2	of	of	ADP
eurjchem-1252	123	3	3,3‐dibromo‐7,8,9‐triphenyl‐2h‐pyrimido	3,3‐dibromo‐7,8,9‐triphenyl‐2h‐pyrimido	NUM
eurjchem-1252	124	1	[	[	X
eurjchem-1252	124	2	1,2‐b]pyridazine‐2,4(3h)‐dione	1,2‐b]pyridazine‐2,4(3h)‐dione	NUM
eurjchem-1252	124	3	(	(	PUNCT
eurjchem-1252	124	4	5	5	NUM
eurjchem-1252	124	5	)	)	PUNCT
eurjchem-1252	124	6	to	to	ADP
eurjchem-1252	124	7	a	a	DET
eurjchem-1252	124	8	solution	solution	NOUN
eurjchem-1252	124	9	of	of	ADP
eurjchem-1252	124	10	compound	compound	NOUN
eurjchem-1252	124	11	1	1	NUM
eurjchem-1252	124	12	(	(	PUNCT
eurjchem-1252	124	13	0.5	0.5	NUM
eurjchem-1252	124	14	g	g	NOUN
eurjchem-1252	124	15	,	,	PUNCT
eurjchem-1252	124	16	1.28	1.28	NUM
eurjchem-1252	124	17	mmol	mmol	NOUN
eurjchem-1252	124	18	)	)	PUNCT
eurjchem-1252	124	19	in	in	ADP
eurjchem-1252	124	20	chloroform	chloroform	NOUN
eurjchem-1252	124	21	(	(	PUNCT
eurjchem-1252	124	22	10	10	NUM
eurjchem-1252	124	23	ml	ml	NOUN
eurjchem-1252	124	24	)	)	PUNCT
eurjchem-1252	124	25	,	,	PUNCT
eurjchem-1252	124	26	bromine	bromine	NOUN
eurjchem-1252	124	27	(	(	PUNCT
eurjchem-1252	124	28	2.56	2.56	NUM
eurjchem-1252	124	29	mmol	mmol	NOUN
eurjchem-1252	124	30	)	)	PUNCT
eurjchem-1252	124	31	was	be	AUX
eurjchem-1252	124	32	added	add	VERB
eurjchem-1252	124	33	,	,	PUNCT
eurjchem-1252	124	34	and	and	CCONJ
eurjchem-1252	124	35	the	the	DET
eurjchem-1252	124	36	reaction	reaction	NOUN
eurjchem-1252	124	37	mixture	mixture	NOUN
eurjchem-1252	124	38	was	be	AUX
eurjchem-1252	124	39	stirred	stir	VERB
eurjchem-1252	124	40	at	at	ADP
eurjchem-1252	124	41	room	room	NOUN
eurjchem-1252	124	42	temperature	temperature	NOUN
eurjchem-1252	124	43	for	for	ADP
eurjchem-1252	124	44	2	2	NUM
eurjchem-1252	124	45	h.	h.	NOUN
eurjchem-1252	124	46	the	the	DET
eurjchem-1252	124	47	solvent	solvent	NOUN
eurjchem-1252	124	48	was	be	AUX
eurjchem-1252	124	49	evaporated	evaporate	VERB
eurjchem-1252	124	50	,	,	PUNCT
eurjchem-1252	124	51	and	and	CCONJ
eurjchem-1252	124	52	the	the	DET
eurjchem-1252	124	53	residue	residue	NOUN
eurjchem-1252	124	54	was	be	AUX
eurjchem-1252	124	55	triturated	triturate	VERB
eurjchem-1252	124	56	with	with	ADP
eurjchem-1252	124	57	water	water	NOUN
eurjchem-1252	124	58	.	.	PUNCT
eurjchem-1252	125	1	the	the	DET
eurjchem-1252	125	2	solid	solid	ADJ
eurjchem-1252	125	3	product	product	NOUN
eurjchem-1252	125	4	was	be	AUX
eurjchem-1252	125	5	filtered	filter	VERB
eurjchem-1252	125	6	off	off	ADP
eurjchem-1252	125	7	,	,	PUNCT
eurjchem-1252	125	8	washed	wash	VERB
eurjchem-1252	125	9	with	with	ADP
eurjchem-1252	125	10	water	water	NOUN
eurjchem-1252	125	11	,	,	PUNCT
eurjchem-1252	125	12	dried	dry	VERB
eurjchem-1252	125	13	,	,	PUNCT
eurjchem-1252	125	14	and	and	CCONJ
eurjchem-1252	125	15	recrystallized	recrystallize	VERB
eurjchem-1252	125	16	from	from	ADP
eurjchem-1252	125	17	methanol	methanol	NOUN
eurjchem-1252	125	18	to	to	PART
eurjchem-1252	125	19	give	give	VERB
eurjchem-1252	125	20	compound	compound	NOUN
eurjchem-1252	125	21	5	5	NUM
eurjchem-1252	125	22	(	(	PUNCT
eurjchem-1252	125	23	scheme	scheme	NOUN
eurjchem-1252	125	24	2	2	NUM
eurjchem-1252	125	25	)	)	PUNCT
eurjchem-1252	125	26	.	.	PUNCT
eurjchem-1252	126	1	color	color	NOUN
eurjchem-1252	126	2	:	:	PUNCT
eurjchem-1252	126	3	brown	brown	ADJ
eurjchem-1252	126	4	.	.	PUNCT
eurjchem-1252	127	1	yield	yield	NOUN
eurjchem-1252	127	2	:	:	PUNCT
eurjchem-1252	127	3	68.41	68.41	NUM
eurjchem-1252	127	4	%	%	NOUN
eurjchem-1252	127	5	.	.	PUNCT
eurjchem-1252	128	1	m.p	m.p	PROPN
eurjchem-1252	128	2	.	.	PROPN
eurjchem-1252	128	3	:	:	PUNCT
eurjchem-1252	129	1	118‐120	118‐120	NUM
eurjchem-1252	130	1	°	°	PROPN
eurjchem-1252	130	2	c	c	X
eurjchem-1252	130	3	.	.	PUNCT
eurjchem-1252	131	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	131	2	(	(	PUNCT
eurjchem-1252	131	3	kbr	kbr	PROPN
eurjchem-1252	131	4	,	,	PUNCT
eurjchem-1252	131	5	ν	ν	PROPN
eurjchem-1252	131	6	,	,	PUNCT
eurjchem-1252	131	7	cm‐1	cm‐1	PROPN
eurjchem-1252	131	8	):	):	PUNCT
eurjchem-1252	131	9	3056	3056	NUM
eurjchem-1252	131	10	(	(	PUNCT
eurjchem-1252	131	11	ch	ch	NOUN
eurjchem-1252	131	12	,	,	PUNCT
eurjchem-1252	131	13	arom	arom	NOUN
eurjchem-1252	131	14	.	.	PUNCT
eurjchem-1252	131	15	)	)	PUNCT
eurjchem-1252	131	16	,	,	PUNCT
eurjchem-1252	131	17	1710	1710	NUM
eurjchem-1252	131	18	(	(	PUNCT
eurjchem-1252	131	19	c	c	NOUN
eurjchem-1252	131	20	=	=	NOUN
eurjchem-1252	131	21	o	o	NOUN
eurjchem-1252	131	22	)	)	PUNCT
eurjchem-1252	131	23	,	,	PUNCT
eurjchem-1252	131	24	1637	1637	NUM
eurjchem-1252	131	25	(	(	PUNCT
eurjchem-1252	131	26	c	c	NOUN
eurjchem-1252	131	27	=	=	SYM
eurjchem-1252	131	28	n	n	NUM
eurjchem-1252	131	29	)	)	PUNCT
eurjchem-1252	131	30	.	.	PUNCT
eurjchem-1252	132	1	1h	1h	NUM
eurjchem-1252	132	2	nmr	nmr	NOUN
eurjchem-1252	132	3	(	(	PUNCT
eurjchem-1252	132	4	300	300	NUM
eurjchem-1252	132	5	mhz	mhz	NOUN
eurjchem-1252	132	6	,	,	PUNCT
eurjchem-1252	132	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1252	132	8	,	,	PUNCT
eurjchem-1252	132	9	δ	δ	PROPN
eurjchem-1252	132	10	,	,	PUNCT
eurjchem-1252	132	11	ppm	ppm	NUM
eurjchem-1252	132	12	):	):	PUNCT
eurjchem-1252	132	13	6.96‐7.65	6.96‐7.65	NUM
eurjchem-1252	132	14	(	(	PUNCT
eurjchem-1252	132	15	m	m	PROPN
eurjchem-1252	132	16	,	,	PUNCT
eurjchem-1252	132	17	15h	15h	NUM
eurjchem-1252	132	18	,	,	PUNCT
eurjchem-1252	132	19	3ph	3ph	NOUN
eurjchem-1252	132	20	)	)	PUNCT
eurjchem-1252	132	21	.	.	PUNCT
eurjchem-1252	133	1	ms	ms	NOUN
eurjchem-1252	133	2	(	(	PUNCT
eurjchem-1252	133	3	ei	ei	PROPN
eurjchem-1252	133	4	,	,	PUNCT
eurjchem-1252	133	5	m	m	PROPN
eurjchem-1252	133	6	/	/	SYM
eurjchem-1252	133	7	z	z	PROPN
eurjchem-1252	133	8	(	(	PUNCT
eurjchem-1252	133	9	%	%	NOUN
eurjchem-1252	133	10	)	)	PUNCT
eurjchem-1252	133	11	):	):	PUNCT
eurjchem-1252	133	12	549	549	NUM
eurjchem-1252	133	13	(	(	PUNCT
eurjchem-1252	133	14	m+	m+	NUM
eurjchem-1252	133	15	,	,	PUNCT
eurjchem-1252	133	16	30.60	30.60	NUM
eurjchem-1252	133	17	)	)	PUNCT
eurjchem-1252	133	18	,	,	PUNCT
eurjchem-1252	133	19	520	520	NUM
eurjchem-1252	133	20	(	(	PUNCT
eurjchem-1252	133	21	21.35	21.35	NUM
eurjchem-1252	133	22	)	)	PUNCT
eurjchem-1252	133	23	,	,	PUNCT
eurjchem-1252	133	24	508	508	NUM
eurjchem-1252	133	25	(	(	PUNCT
eurjchem-1252	133	26	34.52	34.52	NUM
eurjchem-1252	133	27	)	)	PUNCT
eurjchem-1252	133	28	,	,	PUNCT
eurjchem-1252	133	29	469	469	NUM
eurjchem-1252	133	30	(	(	PUNCT
eurjchem-1252	133	31	23.13	23.13	NUM
eurjchem-1252	133	32	)	)	PUNCT
eurjchem-1252	133	33	,	,	PUNCT
eurjchem-1252	133	34	388	388	NUM
eurjchem-1252	133	35	(	(	PUNCT
eurjchem-1252	133	36	23.13	23.13	NUM
eurjchem-1252	133	37	)	)	PUNCT
eurjchem-1252	133	38	,	,	PUNCT
eurjchem-1252	133	39	377	377	NUM
eurjchem-1252	133	40	(	(	PUNCT
eurjchem-1252	133	41	19.57	19.57	NUM
eurjchem-1252	133	42	)	)	PUNCT
eurjchem-1252	133	43	,	,	PUNCT
eurjchem-1252	133	44	372	372	NUM
eurjchem-1252	133	45	(	(	PUNCT
eurjchem-1252	133	46	22.06	22.06	NUM
eurjchem-1252	133	47	)	)	PUNCT
eurjchem-1252	133	48	,	,	PUNCT
eurjchem-1252	133	49	357	357	NUM
eurjchem-1252	133	50	(	(	PUNCT
eurjchem-1252	133	51	20.64	20.64	NUM
eurjchem-1252	133	52	)	)	PUNCT
eurjchem-1252	133	53	,	,	PUNCT
eurjchem-1252	133	54	193	193	NUM
eurjchem-1252	133	55	(	(	PUNCT
eurjchem-1252	133	56	6.76	6.76	NUM
eurjchem-1252	133	57	)	)	PUNCT
eurjchem-1252	133	58	,	,	PUNCT
eurjchem-1252	133	59	172	172	NUM
eurjchem-1252	133	60	(	(	PUNCT
eurjchem-1252	133	61	24.20	24.20	NUM
eurjchem-1252	133	62	)	)	PUNCT
eurjchem-1252	133	63	,	,	PUNCT
eurjchem-1252	133	64	160	160	NUM
eurjchem-1252	133	65	(	(	PUNCT
eurjchem-1252	133	66	25.27	25.27	NUM
eurjchem-1252	133	67	)	)	PUNCT
eurjchem-1252	133	68	,	,	PUNCT
eurjchem-1252	133	69	80	80	NUM
eurjchem-1252	133	70	(	(	PUNCT
eurjchem-1252	133	71	100	100	NUM
eurjchem-1252	133	72	)	)	PUNCT
eurjchem-1252	133	73	.	.	PUNCT
eurjchem-1252	134	1	anal	anal	PROPN
eurjchem-1252	134	2	.	.	PUNCT
eurjchem-1252	134	3	calcd	calcd	NOUN
eurjchem-1252	134	4	.	.	PUNCT
eurjchem-1252	135	1	for	for	ADP
eurjchem-1252	135	2	c25h15br2n3o2	c25h15br2n3o2	PROPN
eurjchem-1252	135	3	:	:	PUNCT
eurjchem-1252	135	4	c	c	X
eurjchem-1252	135	5	,	,	PUNCT
eurjchem-1252	135	6	54.67	54.67	NUM
eurjchem-1252	135	7	;	;	PUNCT
eurjchem-1252	135	8	h	h	NOUN
eurjchem-1252	135	9	,	,	PUNCT
eurjchem-1252	135	10	2.75	2.75	NUM
eurjchem-1252	135	11	;	;	PUNCT
eurjchem-1252	135	12	n	n	CCONJ
eurjchem-1252	135	13	,	,	PUNCT
eurjchem-1252	135	14	7.65	7.65	NUM
eurjchem-1252	135	15	.	.	PUNCT
eurjchem-1252	135	16	found	find	VERB
eurjchem-1252	135	17	:	:	PUNCT
eurjchem-1252	136	1	c	c	X
eurjchem-1252	136	2	,	,	PUNCT
eurjchem-1252	136	3	55.03	55.03	NUM
eurjchem-1252	136	4	;	;	PUNCT
eurjchem-1252	137	1	h	h	NOUN
eurjchem-1252	137	2	,	,	PUNCT
eurjchem-1252	137	3	2.86	2.86	NUM
eurjchem-1252	137	4	;	;	PUNCT
eurjchem-1252	137	5	n	n	CCONJ
eurjchem-1252	137	6	,	,	PUNCT
eurjchem-1252	137	7	7.51	7.51	NUM
eurjchem-1252	137	8	%	%	NOUN
eurjchem-1252	137	9	.	.	PUNCT
eurjchem-1252	138	1	2.2.9	2.2.9	X
eurjchem-1252	138	2	.	.	PUNCT
eurjchem-1252	139	1	synthesis	synthesis	NOUN
eurjchem-1252	139	2	of	of	ADP
eurjchem-1252	139	3	3,3‐dichloro‐7,8,9‐triphenyl‐2h‐pyrimido	3,3‐dichloro‐7,8,9‐triphenyl‐2h‐pyrimido	NOUN
eurjchem-1252	140	1	[	[	X
eurjchem-1252	140	2	1,2‐b]pyridazine‐2,4(3h)‐dione	1,2‐b]pyridazine‐2,4(3h)‐dione	NUM
eurjchem-1252	140	3	(	(	PUNCT
eurjchem-1252	140	4	6	6	NUM
eurjchem-1252	140	5	)	)	PUNCT
eurjchem-1252	140	6	a	a	DET
eurjchem-1252	140	7	solution	solution	NOUN
eurjchem-1252	140	8	of	of	ADP
eurjchem-1252	140	9	compound	compound	NOUN
eurjchem-1252	140	10	1	1	NUM
eurjchem-1252	140	11	(	(	PUNCT
eurjchem-1252	140	12	0.5	0.5	NUM
eurjchem-1252	140	13	g	g	NOUN
eurjchem-1252	140	14	,	,	PUNCT
eurjchem-1252	140	15	1.28	1.28	NUM
eurjchem-1252	140	16	mmol	mmol	NOUN
eurjchem-1252	140	17	)	)	PUNCT
eurjchem-1252	140	18	in	in	ADP
eurjchem-1252	140	19	sulfuryl	sulfuryl	PROPN
eurjchem-1252	140	20	chloride	chloride	PROPN
eurjchem-1252	140	21	(	(	PUNCT
eurjchem-1252	140	22	10	10	NUM
eurjchem-1252	140	23	ml	ml	NOUN
eurjchem-1252	140	24	)	)	PUNCT
eurjchem-1252	140	25	was	be	AUX
eurjchem-1252	140	26	refluxed	refluxe	VERB
eurjchem-1252	140	27	for	for	ADP
eurjchem-1252	140	28	30	30	NUM
eurjchem-1252	140	29	min	min	NOUN
eurjchem-1252	140	30	.	.	PUNCT
eurjchem-1252	141	1	the	the	DET
eurjchem-1252	141	2	reaction	reaction	NOUN
eurjchem-1252	141	3	mixture	mixture	NOUN
eurjchem-1252	141	4	was	be	AUX
eurjchem-1252	141	5	cooled	cool	VERB
eurjchem-1252	141	6	,	,	PUNCT
eurjchem-1252	141	7	poured	pour	VERB
eurjchem-1252	141	8	into	into	ADP
eurjchem-1252	141	9	ice	ice	NOUN
eurjchem-1252	141	10	cold	cold	ADJ
eurjchem-1252	141	11	water	water	NOUN
eurjchem-1252	141	12	(	(	PUNCT
eurjchem-1252	141	13	100	100	NUM
eurjchem-1252	141	14	ml	ml	NOUN
eurjchem-1252	141	15	)	)	PUNCT
eurjchem-1252	141	16	,	,	PUNCT
eurjchem-1252	141	17	and	and	CCONJ
eurjchem-1252	141	18	the	the	DET
eurjchem-1252	141	19	precipitate	precipitate	NOUN
eurjchem-1252	141	20	was	be	AUX
eurjchem-1252	141	21	filtered	filter	VERB
eurjchem-1252	141	22	off	off	ADP
eurjchem-1252	141	23	,	,	PUNCT
eurjchem-1252	141	24	washed	wash	VERB
eurjchem-1252	141	25	with	with	ADP
eurjchem-1252	141	26	water	water	NOUN
eurjchem-1252	141	27	,	,	PUNCT
eurjchem-1252	141	28	dried	dry	VERB
eurjchem-1252	141	29	,	,	PUNCT
eurjchem-1252	141	30	and	and	CCONJ
eurjchem-1252	141	31	recrystallized	recrystallize	VERB
eurjchem-1252	141	32	from	from	ADP
eurjchem-1252	141	33	ethanol	ethanol	NOUN
eurjchem-1252	141	34	to	to	PART
eurjchem-1252	141	35	give	give	VERB
eurjchem-1252	141	36	compound	compound	NOUN
eurjchem-1252	141	37	6	6	NUM
eurjchem-1252	141	38	(	(	PUNCT
eurjchem-1252	141	39	scheme	scheme	NOUN
eurjchem-1252	141	40	2	2	NUM
eurjchem-1252	141	41	)	)	PUNCT
eurjchem-1252	141	42	.	.	PUNCT
eurjchem-1252	142	1	color	color	NOUN
eurjchem-1252	142	2	:	:	PUNCT
eurjchem-1252	142	3	yellow	yellow	ADJ
eurjchem-1252	142	4	.	.	PUNCT
eurjchem-1252	143	1	yield	yield	NOUN
eurjchem-1252	143	2	:	:	PUNCT
eurjchem-1252	143	3	73.13	73.13	NUM
eurjchem-1252	143	4	%	%	NOUN
eurjchem-1252	143	5	.	.	PUNCT
eurjchem-1252	144	1	m.p	m.p	PROPN
eurjchem-1252	144	2	.	.	PROPN
eurjchem-1252	144	3	:	:	PUNCT
eurjchem-1252	145	1	119‐120	119‐120	NUM
eurjchem-1252	145	2	°	°	ADP
eurjchem-1252	145	3	c	c	X
eurjchem-1252	145	4	.	.	PUNCT
eurjchem-1252	145	5	ft‐ir	ft‐ir	NOUN
eurjchem-1252	145	6	(	(	PUNCT
eurjchem-1252	145	7	kbr	kbr	PROPN
eurjchem-1252	145	8	,	,	PUNCT
eurjchem-1252	145	9	ν	ν	PROPN
eurjchem-1252	145	10	,	,	PUNCT
eurjchem-1252	145	11	cm‐1	cm‐1	PROPN
eurjchem-1252	145	12	):	):	PUNCT
eurjchem-1252	145	13	3056	3056	NUM
eurjchem-1252	145	14	(	(	PUNCT
eurjchem-1252	145	15	ch	ch	NOUN
eurjchem-1252	145	16	,	,	PUNCT
eurjchem-1252	145	17	arom	arom	NOUN
eurjchem-1252	145	18	.	.	PUNCT
eurjchem-1252	145	19	)	)	PUNCT
eurjchem-1252	145	20	,	,	PUNCT
eurjchem-1252	145	21	1713	1713	NUM
eurjchem-1252	145	22	(	(	PUNCT
eurjchem-1252	145	23	c	c	NOUN
eurjchem-1252	145	24	=	=	NOUN
eurjchem-1252	145	25	o	o	NOUN
eurjchem-1252	145	26	)	)	PUNCT
eurjchem-1252	145	27	,	,	PUNCT
eurjchem-1252	145	28	1643	1643	NUM
eurjchem-1252	145	29	(	(	PUNCT
eurjchem-1252	145	30	c	c	NOUN
eurjchem-1252	145	31	=	=	SYM
eurjchem-1252	145	32	n	n	NUM
eurjchem-1252	145	33	)	)	PUNCT
eurjchem-1252	145	34	.	.	PUNCT
eurjchem-1252	146	1	1h	1h	NUM
eurjchem-1252	146	2	nmr	nmr	NOUN
eurjchem-1252	146	3	(	(	PUNCT
eurjchem-1252	146	4	300	300	NUM
eurjchem-1252	146	5	mhz	mhz	NOUN
eurjchem-1252	146	6	,	,	PUNCT
eurjchem-1252	146	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1252	146	8	,	,	PUNCT
eurjchem-1252	146	9	δ	δ	PROPN
eurjchem-1252	146	10	,	,	PUNCT
eurjchem-1252	146	11	ppm	ppm	NOUN
eurjchem-1252	146	12	):	):	PUNCT
eurjchem-1252	146	13	7.23‐7.62	7.23‐7.62	NUM
eurjchem-1252	146	14	(	(	PUNCT
eurjchem-1252	146	15	m	m	PROPN
eurjchem-1252	146	16	,	,	PUNCT
eurjchem-1252	146	17	15h	15h	NUM
eurjchem-1252	146	18	,	,	PUNCT
eurjchem-1252	146	19	3ph	3ph	NOUN
eurjchem-1252	146	20	)	)	PUNCT
eurjchem-1252	146	21	.	.	PUNCT
eurjchem-1252	147	1	ms	ms	NOUN
eurjchem-1252	147	2	(	(	PUNCT
eurjchem-1252	147	3	ei	ei	PROPN
eurjchem-1252	147	4	,	,	PUNCT
eurjchem-1252	147	5	m	m	PROPN
eurjchem-1252	147	6	/	/	SYM
eurjchem-1252	147	7	z	z	PROPN
eurjchem-1252	147	8	(	(	PUNCT
eurjchem-1252	147	9	%	%	NOUN
eurjchem-1252	147	10	)	)	PUNCT
eurjchem-1252	147	11	):	):	PUNCT
eurjchem-1252	147	12	460	460	NUM
eurjchem-1252	147	13	(	(	PUNCT
eurjchem-1252	147	14	m+	m+	NUM
eurjchem-1252	147	15	,	,	PUNCT
eurjchem-1252	147	16	62.86	62.86	NUM
eurjchem-1252	147	17	)	)	PUNCT
eurjchem-1252	147	18	,	,	PUNCT
eurjchem-1252	147	19	417	417	NUM
eurjchem-1252	147	20	(	(	PUNCT
eurjchem-1252	147	21	77.14	77.14	NUM
eurjchem-1252	147	22	)	)	PUNCT
eurjchem-1252	147	23	,	,	PUNCT
eurjchem-1252	147	24	384	384	NUM
eurjchem-1252	147	25	(	(	PUNCT
eurjchem-1252	147	26	64.76	64.76	NUM
eurjchem-1252	147	27	)	)	PUNCT
eurjchem-1252	147	28	,	,	PUNCT
eurjchem-1252	147	29	377	377	NUM
eurjchem-1252	147	30	(	(	PUNCT
eurjchem-1252	147	31	57.14	57.14	NUM
eurjchem-1252	147	32	)	)	PUNCT
eurjchem-1252	147	33	,	,	PUNCT
eurjchem-1252	147	34	284	284	NUM
eurjchem-1252	147	35	(	(	PUNCT
eurjchem-1252	147	36	72.38	72.38	NUM
eurjchem-1252	147	37	)	)	PUNCT
eurjchem-1252	147	38	,	,	PUNCT
eurjchem-1252	147	39	230	230	NUM
eurjchem-1252	147	40	(	(	PUNCT
eurjchem-1252	147	41	64.76	64.76	NUM
eurjchem-1252	147	42	)	)	PUNCT
eurjchem-1252	147	43	,	,	PUNCT
eurjchem-1252	147	44	176	176	NUM
eurjchem-1252	147	45	(	(	PUNCT
eurjchem-1252	147	46	100	100	NUM
eurjchem-1252	147	47	)	)	PUNCT
eurjchem-1252	147	48	,	,	PUNCT
eurjchem-1252	147	49	154	154	NUM
eurjchem-1252	147	50	(	(	PUNCT
eurjchem-1252	147	51	15.24	15.24	NUM
eurjchem-1252	147	52	)	)	PUNCT
eurjchem-1252	147	53	,	,	PUNCT
eurjchem-1252	147	54	126	126	NUM
eurjchem-1252	147	55	(	(	PUNCT
eurjchem-1252	147	56	33.33	33.33	NUM
eurjchem-1252	147	57	)	)	PUNCT
eurjchem-1252	147	58	,	,	PUNCT
eurjchem-1252	147	59	83	83	NUM
eurjchem-1252	147	60	(	(	PUNCT
eurjchem-1252	147	61	66.67	66.67	NUM
eurjchem-1252	147	62	)	)	PUNCT
eurjchem-1252	147	63	.	.	PUNCT
eurjchem-1252	148	1	anal	anal	PROPN
eurjchem-1252	148	2	.	.	PUNCT
eurjchem-1252	148	3	calcd	calcd	NOUN
eurjchem-1252	148	4	.	.	PUNCT
eurjchem-1252	149	1	for	for	SCONJ
eurjchem-1252	149	2	c25h15cl2n3o2	c25h15cl2n3o2	PROPN
eurjchem-1252	149	3	:	:	PUNCT
eurjchem-1252	149	4	c	c	X
eurjchem-1252	149	5	,	,	PUNCT
eurjchem-1252	149	6	65.23	65.23	NUM
eurjchem-1252	149	7	;	;	PUNCT
eurjchem-1252	149	8	h	h	NOUN
eurjchem-1252	149	9	,	,	PUNCT
eurjchem-1252	149	10	3.28	3.28	NUM
eurjchem-1252	149	11	;	;	PUNCT
eurjchem-1252	149	12	n	n	CCONJ
eurjchem-1252	149	13	,	,	PUNCT
eurjchem-1252	149	14	9.13	9.13	NUM
eurjchem-1252	149	15	.	.	PUNCT
eurjchem-1252	149	16	found	find	VERB
eurjchem-1252	149	17	:	:	PUNCT
eurjchem-1252	150	1	c	c	X
eurjchem-1252	150	2	,	,	PUNCT
eurjchem-1252	150	3	65.51	65.51	NUM
eurjchem-1252	150	4	;	;	PUNCT
eurjchem-1252	150	5	h	h	NOUN
eurjchem-1252	150	6	,	,	PUNCT
eurjchem-1252	150	7	3.18	3.18	NUM
eurjchem-1252	150	8	;	;	PUNCT
eurjchem-1252	150	9	n	n	CCONJ
eurjchem-1252	150	10	,	,	PUNCT
eurjchem-1252	150	11	8.99	8.99	NUM
eurjchem-1252	150	12	%	%	NOUN
eurjchem-1252	150	13	.	.	PUNCT
eurjchem-1252	151	1	2.2.10	2.2.10	NUM
eurjchem-1252	151	2	.	.	PUNCT
eurjchem-1252	152	1	synthesis	synthesis	NOUN
eurjchem-1252	152	2	of	of	ADP
eurjchem-1252	152	3	3‐chloro‐6,7,8‐triphenylimidazo[1,2‐b	3‐chloro‐6,7,8‐triphenylimidazo[1,2‐b	NUM
eurjchem-1252	152	4	]	]	X
eurjchem-1252	152	5	pyridazin‐2(3h)‐one	pyridazin‐2(3h)‐one	PROPN
eurjchem-1252	152	6	(	(	PUNCT
eurjchem-1252	152	7	7	7	NUM
eurjchem-1252	152	8	)	)	PUNCT
eurjchem-1252	152	9	a	a	DET
eurjchem-1252	152	10	mixture	mixture	NOUN
eurjchem-1252	152	11	of	of	ADP
eurjchem-1252	152	12	compound	compound	NOUN
eurjchem-1252	152	13	6	6	NUM
eurjchem-1252	152	14	(	(	PUNCT
eurjchem-1252	152	15	0.5	0.5	NUM
eurjchem-1252	152	16	g	g	NOUN
eurjchem-1252	152	17	,	,	PUNCT
eurjchem-1252	152	18	1.09	1.09	NUM
eurjchem-1252	152	19	mmol	mmol	NOUN
eurjchem-1252	152	20	)	)	PUNCT
eurjchem-1252	152	21	in	in	ADP
eurjchem-1252	152	22	aq	aq	PROPN
eurjchem-1252	152	23	.	.	PROPN
eurjchem-1252	152	24	sodium	sodium	NOUN
eurjchem-1252	152	25	carbonate	carbonate	NOUN
eurjchem-1252	152	26	solution	solution	NOUN
eurjchem-1252	152	27	was	be	AUX
eurjchem-1252	152	28	refluxed	refluxe	VERB
eurjchem-1252	152	29	for	for	ADP
eurjchem-1252	152	30	6	6	NUM
eurjchem-1252	152	31	h.	h.	NOUN
eurjchem-1252	152	32	after	after	ADP
eurjchem-1252	152	33	cooling	cool	VERB
eurjchem-1252	152	34	,	,	PUNCT
eurjchem-1252	152	35	the	the	DET
eurjchem-1252	152	36	deeb	deeb	PROPN
eurjchem-1252	152	37	et	et	PROPN
eurjchem-1252	152	38	al	al	PROPN
eurjchem-1252	152	39	.	.	PUNCT
eurjchem-1252	152	40	/	/	SYM
eurjchem-1252	152	41	european	european	PROPN
eurjchem-1252	152	42	journal	journal	PROPN
eurjchem-1252	152	43	of	of	ADP
eurjchem-1252	152	44	chemistry	chemistry	NOUN
eurjchem-1252	152	45	6	6	NUM
eurjchem-1252	152	46	(	(	PUNCT
eurjchem-1252	152	47	2	2	NUM
eurjchem-1252	152	48	)	)	PUNCT
eurjchem-1252	152	49	(	(	PUNCT
eurjchem-1252	152	50	2015	2015	NUM
eurjchem-1252	152	51	)	)	PUNCT
eurjchem-1252	153	1	204‐210	204‐210	PROPN
eurjchem-1252	153	2	207	207	NUM
eurjchem-1252	153	3	reaction	reaction	NOUN
eurjchem-1252	153	4	mixture	mixture	NOUN
eurjchem-1252	153	5	was	be	AUX
eurjchem-1252	153	6	filtered	filter	VERB
eurjchem-1252	153	7	off	off	ADP
eurjchem-1252	153	8	.	.	PUNCT
eurjchem-1252	154	1	the	the	DET
eurjchem-1252	154	2	residue	residue	NOUN
eurjchem-1252	154	3	was	be	AUX
eurjchem-1252	154	4	triturated	triturate	VERB
eurjchem-1252	154	5	with	with	ADP
eurjchem-1252	154	6	water	water	NOUN
eurjchem-1252	154	7	,	,	PUNCT
eurjchem-1252	154	8	filtered	filter	VERB
eurjchem-1252	154	9	off	off	ADP
eurjchem-1252	154	10	,	,	PUNCT
eurjchem-1252	154	11	dried	dry	VERB
eurjchem-1252	154	12	,	,	PUNCT
eurjchem-1252	154	13	and	and	CCONJ
eurjchem-1252	154	14	recrystallized	recrystallize	VERB
eurjchem-1252	154	15	from	from	ADP
eurjchem-1252	154	16	ethanol	ethanol	NOUN
eurjchem-1252	154	17	to	to	PART
eurjchem-1252	154	18	give	give	VERB
eurjchem-1252	154	19	compound	compound	NOUN
eurjchem-1252	154	20	7	7	NUM
eurjchem-1252	154	21	(	(	PUNCT
eurjchem-1252	154	22	scheme	scheme	NOUN
eurjchem-1252	154	23	2	2	NUM
eurjchem-1252	154	24	)	)	PUNCT
eurjchem-1252	154	25	.	.	PUNCT
eurjchem-1252	155	1	color	color	NOUN
eurjchem-1252	155	2	:	:	PUNCT
eurjchem-1252	155	3	brown	brown	ADJ
eurjchem-1252	155	4	.	.	PUNCT
eurjchem-1252	156	1	yield	yield	NOUN
eurjchem-1252	156	2	:	:	PUNCT
eurjchem-1252	156	3	53.23	53.23	NUM
eurjchem-1252	156	4	%	%	NOUN
eurjchem-1252	156	5	.	.	PUNCT
eurjchem-1252	157	1	m.p	m.p	PROPN
eurjchem-1252	157	2	.	.	PROPN
eurjchem-1252	157	3	:	:	PUNCT
eurjchem-1252	157	4	215‐217	215‐217	NUM
eurjchem-1252	157	5	°	°	PROPN
eurjchem-1252	157	6	c	c	NOUN
eurjchem-1252	157	7	.	.	PUNCT
eurjchem-1252	158	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	158	2	(	(	PUNCT
eurjchem-1252	158	3	kbr	kbr	PROPN
eurjchem-1252	158	4	,	,	PUNCT
eurjchem-1252	158	5	ν	ν	PROPN
eurjchem-1252	158	6	,	,	PUNCT
eurjchem-1252	158	7	cm‐1	cm‐1	PROPN
eurjchem-1252	158	8	):	):	PUNCT
eurjchem-1252	158	9	3057	3057	NUM
eurjchem-1252	158	10	(	(	PUNCT
eurjchem-1252	158	11	ch	ch	NOUN
eurjchem-1252	158	12	,	,	PUNCT
eurjchem-1252	158	13	arom	arom	NOUN
eurjchem-1252	158	14	.	.	PUNCT
eurjchem-1252	158	15	)	)	PUNCT
eurjchem-1252	158	16	,	,	PUNCT
eurjchem-1252	158	17	1704	1704	NUM
eurjchem-1252	158	18	(	(	PUNCT
eurjchem-1252	158	19	c	c	NOUN
eurjchem-1252	158	20	=	=	NOUN
eurjchem-1252	158	21	o	o	NOUN
eurjchem-1252	158	22	)	)	PUNCT
eurjchem-1252	158	23	,	,	PUNCT
eurjchem-1252	158	24	1632	1632	NUM
eurjchem-1252	158	25	(	(	PUNCT
eurjchem-1252	158	26	c	c	NOUN
eurjchem-1252	158	27	=	=	SYM
eurjchem-1252	158	28	n	n	NUM
eurjchem-1252	158	29	)	)	PUNCT
eurjchem-1252	158	30	.	.	PUNCT
eurjchem-1252	159	1	1h	1h	NUM
eurjchem-1252	159	2	nmr	nmr	NOUN
eurjchem-1252	159	3	(	(	PUNCT
eurjchem-1252	159	4	300	300	NUM
eurjchem-1252	159	5	mhz	mhz	NOUN
eurjchem-1252	159	6	,	,	PUNCT
eurjchem-1252	159	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1252	159	8	,	,	PUNCT
eurjchem-1252	159	9	δ	δ	PROPN
eurjchem-1252	159	10	,	,	PUNCT
eurjchem-1252	159	11	ppm	ppm	NUM
eurjchem-1252	159	12	):	):	PUNCT
eurjchem-1252	159	13	5.82	5.82	NUM
eurjchem-1252	159	14	(	(	PUNCT
eurjchem-1252	159	15	s	s	PROPN
eurjchem-1252	159	16	,	,	PUNCT
eurjchem-1252	159	17	1h	1h	NUM
eurjchem-1252	159	18	,	,	PUNCT
eurjchem-1252	159	19	ch	ch	NOUN
eurjchem-1252	159	20	,	,	PUNCT
eurjchem-1252	159	21	imidazol	imidazol	ADJ
eurjchem-1252	159	22	ring	ring	NOUN
eurjchem-1252	159	23	)	)	PUNCT
eurjchem-1252	159	24	,	,	PUNCT
eurjchem-1252	159	25	6.89‐7.28	6.89‐7.28	NUM
eurjchem-1252	159	26	(	(	PUNCT
eurjchem-1252	159	27	m	m	PROPN
eurjchem-1252	159	28	,	,	PUNCT
eurjchem-1252	159	29	15h	15h	NUM
eurjchem-1252	159	30	,	,	PUNCT
eurjchem-1252	159	31	3ph	3ph	NOUN
eurjchem-1252	159	32	)	)	PUNCT
eurjchem-1252	159	33	.	.	PUNCT
eurjchem-1252	160	1	ms	ms	NOUN
eurjchem-1252	160	2	(	(	PUNCT
eurjchem-1252	160	3	ei	ei	PROPN
eurjchem-1252	160	4	,	,	PUNCT
eurjchem-1252	160	5	m	m	PROPN
eurjchem-1252	160	6	/	/	SYM
eurjchem-1252	160	7	z	z	PROPN
eurjchem-1252	160	8	(	(	PUNCT
eurjchem-1252	160	9	%	%	NOUN
eurjchem-1252	160	10	)	)	PUNCT
eurjchem-1252	160	11	):	):	PUNCT
eurjchem-1252	160	12	400	400	NUM
eurjchem-1252	160	13	(	(	PUNCT
eurjchem-1252	160	14	m+	m+	NOUN
eurjchem-1252	160	15	+	+	CCONJ
eurjchem-1252	160	16	2	2	NUM
eurjchem-1252	160	17	,	,	PUNCT
eurjchem-1252	160	18	0.02	0.02	NUM
eurjchem-1252	160	19	)	)	PUNCT
eurjchem-1252	160	20	,	,	PUNCT
eurjchem-1252	160	21	398	398	NUM
eurjchem-1252	160	22	(	(	PUNCT
eurjchem-1252	160	23	m+	m+	NUM
eurjchem-1252	160	24	,	,	PUNCT
eurjchem-1252	160	25	0.15	0.15	NUM
eurjchem-1252	160	26	)	)	PUNCT
eurjchem-1252	160	27	,	,	PUNCT
eurjchem-1252	160	28	321	321	NUM
eurjchem-1252	160	29	(	(	PUNCT
eurjchem-1252	160	30	2.10	2.10	NUM
eurjchem-1252	160	31	)	)	PUNCT
eurjchem-1252	160	32	,	,	PUNCT
eurjchem-1252	160	33	307	307	NUM
eurjchem-1252	160	34	(	(	PUNCT
eurjchem-1252	160	35	2.37	2.37	NUM
eurjchem-1252	160	36	)	)	PUNCT
eurjchem-1252	160	37	,	,	PUNCT
eurjchem-1252	160	38	294	294	NUM
eurjchem-1252	160	39	(	(	PUNCT
eurjchem-1252	160	40	2.11	2.11	NUM
eurjchem-1252	160	41	)	)	PUNCT
eurjchem-1252	160	42	,	,	PUNCT
eurjchem-1252	160	43	277	277	NUM
eurjchem-1252	160	44	(	(	PUNCT
eurjchem-1252	160	45	100	100	NUM
eurjchem-1252	160	46	)	)	PUNCT
eurjchem-1252	160	47	,	,	PUNCT
eurjchem-1252	160	48	206	206	NUM
eurjchem-1252	160	49	(	(	PUNCT
eurjchem-1252	160	50	0.30	0.30	NUM
eurjchem-1252	160	51	)	)	PUNCT
eurjchem-1252	160	52	,	,	PUNCT
eurjchem-1252	160	53	192	192	NUM
eurjchem-1252	160	54	(	(	PUNCT
eurjchem-1252	160	55	1.44	1.44	NUM
eurjchem-1252	160	56	)	)	PUNCT
eurjchem-1252	160	57	,	,	PUNCT
eurjchem-1252	160	58	178	178	NUM
eurjchem-1252	160	59	(	(	PUNCT
eurjchem-1252	160	60	10.14	10.14	NUM
eurjchem-1252	160	61	)	)	PUNCT
eurjchem-1252	160	62	,	,	PUNCT
eurjchem-1252	160	63	117	117	NUM
eurjchem-1252	160	64	(	(	PUNCT
eurjchem-1252	160	65	27.40	27.40	NUM
eurjchem-1252	160	66	)	)	PUNCT
eurjchem-1252	160	67	,	,	PUNCT
eurjchem-1252	160	68	103	103	NUM
eurjchem-1252	160	69	(	(	PUNCT
eurjchem-1252	160	70	1.37	1.37	NUM
eurjchem-1252	160	71	)	)	PUNCT
eurjchem-1252	160	72	,	,	PUNCT
eurjchem-1252	160	73	91	91	NUM
eurjchem-1252	160	74	(	(	PUNCT
eurjchem-1252	160	75	1.93	1.93	NUM
eurjchem-1252	160	76	)	)	PUNCT
eurjchem-1252	160	77	,	,	PUNCT
eurjchem-1252	160	78	77	77	NUM
eurjchem-1252	160	79	(	(	PUNCT
eurjchem-1252	160	80	40.94	40.94	NUM
eurjchem-1252	160	81	)	)	PUNCT
eurjchem-1252	160	82	.	.	PUNCT
eurjchem-1252	161	1	anal	anal	PROPN
eurjchem-1252	161	2	.	.	PUNCT
eurjchem-1252	161	3	calcd	calcd	NOUN
eurjchem-1252	161	4	.	.	PUNCT
eurjchem-1252	162	1	for	for	ADP
eurjchem-1252	162	2	c24h16cln3o	c24h16cln3o	NOUN
eurjchem-1252	162	3	:	:	PUNCT
eurjchem-1252	162	4	c	c	X
eurjchem-1252	162	5	,	,	PUNCT
eurjchem-1252	162	6	72.45	72.45	NUM
eurjchem-1252	162	7	;	;	PUNCT
eurjchem-1252	162	8	h	h	NOUN
eurjchem-1252	162	9	,	,	PUNCT
eurjchem-1252	162	10	4.05	4.05	NUM
eurjchem-1252	162	11	;	;	PUNCT
eurjchem-1252	162	12	n	n	CCONJ
eurjchem-1252	162	13	,	,	PUNCT
eurjchem-1252	162	14	10.56	10.56	NUM
eurjchem-1252	162	15	.	.	PUNCT
eurjchem-1252	163	1	found	find	VERB
eurjchem-1252	163	2	:	:	PUNCT
eurjchem-1252	164	1	c	c	X
eurjchem-1252	164	2	,	,	PUNCT
eurjchem-1252	164	3	72.78	72.78	NUM
eurjchem-1252	164	4	;	;	PUNCT
eurjchem-1252	164	5	h	h	NOUN
eurjchem-1252	164	6	,	,	PUNCT
eurjchem-1252	164	7	4.17	4.17	NUM
eurjchem-1252	164	8	;	;	PUNCT
eurjchem-1252	164	9	n	n	CCONJ
eurjchem-1252	164	10	,	,	PUNCT
eurjchem-1252	164	11	10.34	10.34	NUM
eurjchem-1252	164	12	%	%	NOUN
eurjchem-1252	164	13	.	.	PUNCT
eurjchem-1252	165	1	2.2.11	2.2.11	X
eurjchem-1252	165	2	.	.	X
eurjchem-1252	166	1	synthesis	synthesis	NOUN
eurjchem-1252	166	2	of	of	ADP
eurjchem-1252	166	3	3‐chloro‐7,8,9‐triphenyl‐2h‐pyrimido	3‐chloro‐7,8,9‐triphenyl‐2h‐pyrimido	NOUN
eurjchem-1252	166	4	[	[	X
eurjchem-1252	166	5	1,2‐b]pyridazine‐2,4(3h)‐dione	1,2‐b]pyridazine‐2,4(3h)‐dione	NUM
eurjchem-1252	166	6	(	(	PUNCT
eurjchem-1252	166	7	8)	8)	NUM
eurjchem-1252	166	8	a	a	DET
eurjchem-1252	166	9	solution	solution	NOUN
eurjchem-1252	166	10	of	of	ADP
eurjchem-1252	166	11	compound	compound	NOUN
eurjchem-1252	166	12	6	6	NUM
eurjchem-1252	166	13	(	(	PUNCT
eurjchem-1252	166	14	0.5	0.5	NUM
eurjchem-1252	166	15	g	g	NOUN
eurjchem-1252	166	16	,	,	PUNCT
eurjchem-1252	166	17	1.09	1.09	NUM
eurjchem-1252	166	18	mmol	mmol	NOUN
eurjchem-1252	166	19	)	)	PUNCT
eurjchem-1252	166	20	in	in	ADP
eurjchem-1252	166	21	glacial	glacial	ADJ
eurjchem-1252	166	22	acetic	acetic	ADJ
eurjchem-1252	166	23	acid	acid	NOUN
eurjchem-1252	166	24	(	(	PUNCT
eurjchem-1252	166	25	10	10	NUM
eurjchem-1252	166	26	ml	ml	NOUN
eurjchem-1252	166	27	)	)	PUNCT
eurjchem-1252	166	28	in	in	ADP
eurjchem-1252	166	29	presence	presence	NOUN
eurjchem-1252	166	30	of	of	ADP
eurjchem-1252	166	31	zinc	zinc	NOUN
eurjchem-1252	166	32	dust	dust	NOUN
eurjchem-1252	166	33	was	be	AUX
eurjchem-1252	166	34	refluxed	refluxe	VERB
eurjchem-1252	166	35	for	for	ADP
eurjchem-1252	166	36	1.5	1.5	NUM
eurjchem-1252	166	37	h	h	NOUN
eurjchem-1252	166	38	,	,	PUNCT
eurjchem-1252	166	39	then	then	ADV
eurjchem-1252	166	40	filtered	filter	VERB
eurjchem-1252	166	41	on	on	ADP
eurjchem-1252	166	42	hot	hot	ADJ
eurjchem-1252	166	43	.	.	PUNCT
eurjchem-1252	167	1	the	the	DET
eurjchem-1252	167	2	filtrate	filtrate	NOUN
eurjchem-1252	167	3	was	be	AUX
eurjchem-1252	167	4	cooled	cool	VERB
eurjchem-1252	167	5	,	,	PUNCT
eurjchem-1252	167	6	poured	pour	VERB
eurjchem-1252	167	7	into	into	ADP
eurjchem-1252	167	8	water	water	NOUN
eurjchem-1252	167	9	(	(	PUNCT
eurjchem-1252	167	10	100	100	NUM
eurjchem-1252	167	11	ml	ml	NOUN
eurjchem-1252	167	12	)	)	PUNCT
eurjchem-1252	167	13	,	,	PUNCT
eurjchem-1252	167	14	and	and	CCONJ
eurjchem-1252	167	15	the	the	DET
eurjchem-1252	167	16	precipitate	precipitate	NOUN
eurjchem-1252	167	17	was	be	AUX
eurjchem-1252	167	18	filtered	filter	VERB
eurjchem-1252	167	19	off	off	ADP
eurjchem-1252	167	20	,	,	PUNCT
eurjchem-1252	167	21	washed	wash	VERB
eurjchem-1252	167	22	with	with	ADP
eurjchem-1252	167	23	water	water	NOUN
eurjchem-1252	167	24	,	,	PUNCT
eurjchem-1252	167	25	dried	dry	VERB
eurjchem-1252	167	26	,	,	PUNCT
eurjchem-1252	167	27	and	and	CCONJ
eurjchem-1252	167	28	recrystallized	recrystallize	VERB
eurjchem-1252	167	29	from	from	ADP
eurjchem-1252	167	30	acetone	acetone	NOUN
eurjchem-1252	167	31	to	to	PART
eurjchem-1252	167	32	give	give	VERB
eurjchem-1252	167	33	compound	compound	NOUN
eurjchem-1252	167	34	8	8	NUM
eurjchem-1252	167	35	(	(	PUNCT
eurjchem-1252	167	36	scheme	scheme	NOUN
eurjchem-1252	167	37	2	2	NUM
eurjchem-1252	167	38	)	)	PUNCT
eurjchem-1252	167	39	.	.	PUNCT
eurjchem-1252	168	1	color	color	NOUN
eurjchem-1252	168	2	:	:	PUNCT
eurjchem-1252	168	3	colorless	colorless	ADJ
eurjchem-1252	168	4	.	.	PUNCT
eurjchem-1252	169	1	yield	yield	NOUN
eurjchem-1252	169	2	:	:	PUNCT
eurjchem-1252	169	3	69.17	69.17	NUM
eurjchem-1252	169	4	%	%	NOUN
eurjchem-1252	169	5	.	.	PUNCT
eurjchem-1252	170	1	m.p	m.p	PROPN
eurjchem-1252	170	2	.	.	PROPN
eurjchem-1252	170	3	:	:	PUNCT
eurjchem-1252	171	1	160‐162	160‐162	NUM
eurjchem-1252	171	2	°	°	NUM
eurjchem-1252	171	3	c	c	X
eurjchem-1252	171	4	.	.	PUNCT
eurjchem-1252	172	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	172	2	(	(	PUNCT
eurjchem-1252	172	3	kbr	kbr	PROPN
eurjchem-1252	172	4	,	,	PUNCT
eurjchem-1252	172	5	ν	ν	PROPN
eurjchem-1252	172	6	,	,	PUNCT
eurjchem-1252	172	7	cm‐1	cm‐1	PROPN
eurjchem-1252	172	8	):	):	PUNCT
eurjchem-1252	172	9	3057	3057	NUM
eurjchem-1252	172	10	(	(	PUNCT
eurjchem-1252	172	11	ch	ch	NOUN
eurjchem-1252	172	12	,	,	PUNCT
eurjchem-1252	172	13	arom	arom	NOUN
eurjchem-1252	172	14	.	.	PUNCT
eurjchem-1252	172	15	)	)	PUNCT
eurjchem-1252	172	16	,	,	PUNCT
eurjchem-1252	172	17	1704	1704	NUM
eurjchem-1252	172	18	(	(	PUNCT
eurjchem-1252	172	19	c	c	NOUN
eurjchem-1252	172	20	=	=	NOUN
eurjchem-1252	172	21	o	o	NOUN
eurjchem-1252	172	22	)	)	PUNCT
eurjchem-1252	172	23	,	,	PUNCT
eurjchem-1252	172	24	1632	1632	NUM
eurjchem-1252	172	25	(	(	PUNCT
eurjchem-1252	172	26	c	c	NOUN
eurjchem-1252	172	27	=	=	SYM
eurjchem-1252	172	28	n	n	NUM
eurjchem-1252	172	29	)	)	PUNCT
eurjchem-1252	172	30	.	.	PUNCT
eurjchem-1252	173	1	1h	1h	NUM
eurjchem-1252	173	2	nmr	nmr	NOUN
eurjchem-1252	173	3	(	(	PUNCT
eurjchem-1252	173	4	300	300	NUM
eurjchem-1252	173	5	mhz	mhz	NOUN
eurjchem-1252	173	6	,	,	PUNCT
eurjchem-1252	173	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1252	173	8	,	,	PUNCT
eurjchem-1252	173	9	δ	δ	PROPN
eurjchem-1252	173	10	,	,	PUNCT
eurjchem-1252	173	11	ppm	ppm	NUM
eurjchem-1252	173	12	):	):	PUNCT
eurjchem-1252	173	13	5.02	5.02	NUM
eurjchem-1252	173	14	(	(	PUNCT
eurjchem-1252	173	15	s	s	PROPN
eurjchem-1252	173	16	,	,	PUNCT
eurjchem-1252	173	17	1h	1h	NUM
eurjchem-1252	173	18	,	,	PUNCT
eurjchem-1252	173	19	ch	ch	NOUN
eurjchem-1252	173	20	,	,	PUNCT
eurjchem-1252	173	21	pyrimidine	pyrimidine	NOUN
eurjchem-1252	173	22	ring	ring	NOUN
eurjchem-1252	173	23	)	)	PUNCT
eurjchem-1252	173	24	,	,	PUNCT
eurjchem-1252	173	25	7.23‐7.65	7.23‐7.65	NUM
eurjchem-1252	173	26	(	(	PUNCT
eurjchem-1252	173	27	m	m	PROPN
eurjchem-1252	173	28	,	,	PUNCT
eurjchem-1252	173	29	15h	15h	NUM
eurjchem-1252	173	30	,	,	PUNCT
eurjchem-1252	173	31	3ph	3ph	NOUN
eurjchem-1252	173	32	)	)	PUNCT
eurjchem-1252	173	33	.	.	PUNCT
eurjchem-1252	174	1	ms	ms	NOUN
eurjchem-1252	174	2	(	(	PUNCT
eurjchem-1252	174	3	ei	ei	PROPN
eurjchem-1252	174	4	,	,	PUNCT
eurjchem-1252	174	5	m	m	PROPN
eurjchem-1252	174	6	/	/	SYM
eurjchem-1252	174	7	z	z	PROPN
eurjchem-1252	174	8	(	(	PUNCT
eurjchem-1252	174	9	%	%	NOUN
eurjchem-1252	174	10	)	)	PUNCT
eurjchem-1252	174	11	):	):	PUNCT
eurjchem-1252	174	12	427.5	427.5	NUM
eurjchem-1252	174	13	(	(	PUNCT
eurjchem-1252	174	14	m+	m+	NOUN
eurjchem-1252	174	15	+2	+2	NOUN
eurjchem-1252	174	16	,	,	PUNCT
eurjchem-1252	174	17	1.02	1.02	NUM
eurjchem-1252	174	18	)	)	PUNCT
eurjchem-1252	174	19	,	,	PUNCT
eurjchem-1252	174	20	425.5	425.5	NUM
eurjchem-1252	174	21	(	(	PUNCT
eurjchem-1252	174	22	m+	m+	NUM
eurjchem-1252	174	23	,	,	PUNCT
eurjchem-1252	174	24	76.29	76.29	NUM
eurjchem-1252	174	25	)	)	PUNCT
eurjchem-1252	174	26	,	,	PUNCT
eurjchem-1252	174	27	409	409	NUM
eurjchem-1252	174	28	(	(	PUNCT
eurjchem-1252	174	29	86.60	86.60	NUM
eurjchem-1252	174	30	)	)	PUNCT
eurjchem-1252	174	31	,	,	PUNCT
eurjchem-1252	174	32	185	185	NUM
eurjchem-1252	174	33	(	(	PUNCT
eurjchem-1252	174	34	100	100	NUM
eurjchem-1252	174	35	)	)	PUNCT
eurjchem-1252	174	36	.	.	PUNCT
eurjchem-1252	175	1	anal	anal	PROPN
eurjchem-1252	175	2	.	.	PUNCT
eurjchem-1252	175	3	calcd	calcd	NOUN
eurjchem-1252	175	4	.	.	PUNCT
eurjchem-1252	176	1	for	for	SCONJ
eurjchem-1252	176	2	c25h16cln3o2	c25h16cln3o2	NOUN
eurjchem-1252	176	3	:	:	PUNCT
eurjchem-1252	176	4	c	c	X
eurjchem-1252	176	5	,	,	PUNCT
eurjchem-1252	176	6	70.51	70.51	NUM
eurjchem-1252	176	7	;	;	PUNCT
eurjchem-1252	176	8	h	h	NOUN
eurjchem-1252	176	9	,	,	PUNCT
eurjchem-1252	176	10	3.79	3.79	NUM
eurjchem-1252	176	11	;	;	PUNCT
eurjchem-1252	176	12	n	n	CCONJ
eurjchem-1252	176	13	,	,	PUNCT
eurjchem-1252	176	14	9.87	9.87	NUM
eurjchem-1252	176	15	.	.	PUNCT
eurjchem-1252	176	16	found	find	VERB
eurjchem-1252	176	17	:	:	PUNCT
eurjchem-1252	177	1	c	c	X
eurjchem-1252	177	2	,	,	PUNCT
eurjchem-1252	177	3	70.23	70.23	NUM
eurjchem-1252	177	4	;	;	PUNCT
eurjchem-1252	177	5	h	h	NOUN
eurjchem-1252	177	6	,	,	PUNCT
eurjchem-1252	177	7	3.85	3.85	NUM
eurjchem-1252	177	8	;	;	PUNCT
eurjchem-1252	177	9	n	n	CCONJ
eurjchem-1252	177	10	,	,	PUNCT
eurjchem-1252	177	11	10.08	10.08	NUM
eurjchem-1252	177	12	%	%	NOUN
eurjchem-1252	177	13	.	.	PUNCT
eurjchem-1252	178	1	2.2.12	2.2.12	X
eurjchem-1252	178	2	.	.	X
eurjchem-1252	178	3	synthesis	synthesis	NOUN
eurjchem-1252	178	4	of	of	ADP
eurjchem-1252	178	5	3‐amino‐7,8,9‐triphenyl‐2h‐pyrimido	3‐amino‐7,8,9‐triphenyl‐2h‐pyrimido	PRON
eurjchem-1252	178	6	[	[	X
eurjchem-1252	178	7	1,2‐b]pyridazine‐2,4(3h)‐dione	1,2‐b]pyridazine‐2,4(3h)‐dione	NUM
eurjchem-1252	178	8	(	(	PUNCT
eurjchem-1252	178	9	9	9	NUM
eurjchem-1252	178	10	)	)	PUNCT
eurjchem-1252	178	11	method	method	NOUN
eurjchem-1252	178	12	a	a	DET
eurjchem-1252	178	13	:	:	PUNCT
eurjchem-1252	178	14	a	a	DET
eurjchem-1252	178	15	mixture	mixture	NOUN
eurjchem-1252	178	16	of	of	ADP
eurjchem-1252	178	17	compound	compound	NOUN
eurjchem-1252	178	18	8	8	NUM
eurjchem-1252	178	19	(	(	PUNCT
eurjchem-1252	178	20	0.5	0.5	NUM
eurjchem-1252	178	21	g	g	NOUN
eurjchem-1252	178	22	,	,	PUNCT
eurjchem-1252	178	23	1.17	1.17	NUM
eurjchem-1252	178	24	mmol	mmol	NOUN
eurjchem-1252	178	25	)	)	PUNCT
eurjchem-1252	178	26	and	and	CCONJ
eurjchem-1252	178	27	excess	excess	NOUN
eurjchem-1252	178	28	of	of	ADP
eurjchem-1252	178	29	ammonium	ammonium	NOUN
eurjchem-1252	178	30	acetate	acetate	NOUN
eurjchem-1252	178	31	(	(	PUNCT
eurjchem-1252	178	32	3.0	3.0	NUM
eurjchem-1252	178	33	g	g	NOUN
eurjchem-1252	178	34	)	)	PUNCT
eurjchem-1252	178	35	was	be	AUX
eurjchem-1252	178	36	heated	heat	VERB
eurjchem-1252	178	37	in	in	ADP
eurjchem-1252	178	38	a	a	DET
eurjchem-1252	178	39	sand	sand	NOUN
eurjchem-1252	178	40	bath	bath	NOUN
eurjchem-1252	178	41	at	at	ADP
eurjchem-1252	178	42	210	210	NUM
eurjchem-1252	178	43	°	°	ADP
eurjchem-1252	178	44	c	c	NOUN
eurjchem-1252	178	45	for	for	ADP
eurjchem-1252	178	46	30	30	NUM
eurjchem-1252	178	47	min	min	NOUN
eurjchem-1252	178	48	.	.	NOUN
eurjchem-1252	178	49	after	after	ADP
eurjchem-1252	178	50	cooling	cool	VERB
eurjchem-1252	178	51	,	,	PUNCT
eurjchem-1252	178	52	the	the	DET
eurjchem-1252	178	53	solid	solid	ADJ
eurjchem-1252	178	54	product	product	NOUN
eurjchem-1252	178	55	was	be	AUX
eurjchem-1252	178	56	washed	wash	VERB
eurjchem-1252	178	57	with	with	ADP
eurjchem-1252	178	58	water	water	NOUN
eurjchem-1252	178	59	,	,	PUNCT
eurjchem-1252	178	60	filtered	filter	VERB
eurjchem-1252	178	61	off	off	ADP
eurjchem-1252	178	62	,	,	PUNCT
eurjchem-1252	178	63	dried	dry	VERB
eurjchem-1252	178	64	and	and	CCONJ
eurjchem-1252	178	65	recrystallized	recrystallize	VERB
eurjchem-1252	178	66	from	from	ADP
eurjchem-1252	178	67	acetone	acetone	NOUN
eurjchem-1252	178	68	to	to	PART
eurjchem-1252	178	69	give	give	VERB
eurjchem-1252	178	70	compound	compound	NOUN
eurjchem-1252	178	71	9	9	NUM
eurjchem-1252	178	72	(	(	PUNCT
eurjchem-1252	178	73	scheme	scheme	NOUN
eurjchem-1252	178	74	2	2	NUM
eurjchem-1252	178	75	)	)	PUNCT
eurjchem-1252	178	76	.	.	PUNCT
eurjchem-1252	179	1	color	color	NOUN
eurjchem-1252	179	2	:	:	PUNCT
eurjchem-1252	179	3	pale	pale	ADJ
eurjchem-1252	179	4	brown	brown	NOUN
eurjchem-1252	179	5	.	.	PUNCT
eurjchem-1252	180	1	yield	yield	NOUN
eurjchem-1252	180	2	:	:	PUNCT
eurjchem-1252	180	3	58.70	58.70	NUM
eurjchem-1252	180	4	%	%	NOUN
eurjchem-1252	180	5	.	.	PUNCT
eurjchem-1252	181	1	m.p	m.p	PROPN
eurjchem-1252	181	2	.	.	PROPN
eurjchem-1252	181	3	:	:	PUNCT
eurjchem-1252	182	1	128‐130	128‐130	PROPN
eurjchem-1252	182	2	°	°	PROPN
eurjchem-1252	182	3	c	c	PROPN
eurjchem-1252	182	4	.	.	PUNCT
eurjchem-1252	183	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	183	2	(	(	PUNCT
eurjchem-1252	183	3	kbr	kbr	PROPN
eurjchem-1252	183	4	,	,	PUNCT
eurjchem-1252	183	5	ν	ν	PROPN
eurjchem-1252	183	6	,	,	PUNCT
eurjchem-1252	183	7	cm‐1	cm‐1	PROPN
eurjchem-1252	183	8	):	):	PUNCT
eurjchem-1252	183	9	3326	3326	NUM
eurjchem-1252	183	10	,	,	PUNCT
eurjchem-1252	183	11	3188	3188	NUM
eurjchem-1252	183	12	(	(	PUNCT
eurjchem-1252	183	13	nh2	nh2	PROPN
eurjchem-1252	183	14	)	)	PUNCT
eurjchem-1252	183	15	,	,	PUNCT
eurjchem-1252	183	16	3058	3058	NUM
eurjchem-1252	183	17	,	,	PUNCT
eurjchem-1252	183	18	3031	3031	NUM
eurjchem-1252	183	19	(	(	PUNCT
eurjchem-1252	183	20	ch	ch	NOUN
eurjchem-1252	183	21	,	,	PUNCT
eurjchem-1252	183	22	arom	arom	NOUN
eurjchem-1252	183	23	.	.	PUNCT
eurjchem-1252	183	24	)	)	PUNCT
eurjchem-1252	183	25	,	,	PUNCT
eurjchem-1252	183	26	1751	1751	NUM
eurjchem-1252	183	27	,	,	PUNCT
eurjchem-1252	183	28	1681	1681	NUM
eurjchem-1252	183	29	(	(	PUNCT
eurjchem-1252	183	30	c	c	NOUN
eurjchem-1252	183	31	=	=	NOUN
eurjchem-1252	183	32	o	o	NOUN
eurjchem-1252	183	33	)	)	PUNCT
eurjchem-1252	183	34	,	,	PUNCT
eurjchem-1252	183	35	1599	1599	NUM
eurjchem-1252	183	36	(	(	PUNCT
eurjchem-1252	183	37	c	c	NOUN
eurjchem-1252	183	38	=	=	SYM
eurjchem-1252	183	39	n	n	NUM
eurjchem-1252	183	40	)	)	PUNCT
eurjchem-1252	183	41	.	.	PUNCT
eurjchem-1252	184	1	ms	ms	NOUN
eurjchem-1252	184	2	(	(	PUNCT
eurjchem-1252	184	3	ei	ei	PROPN
eurjchem-1252	184	4	,	,	PUNCT
eurjchem-1252	184	5	m	m	PROPN
eurjchem-1252	184	6	/	/	SYM
eurjchem-1252	184	7	z	z	PROPN
eurjchem-1252	184	8	(	(	PUNCT
eurjchem-1252	184	9	%	%	NOUN
eurjchem-1252	184	10	)	)	PUNCT
eurjchem-1252	184	11	):	):	PUNCT
eurjchem-1252	184	12	406	406	NUM
eurjchem-1252	184	13	(	(	PUNCT
eurjchem-1252	184	14	m+	m+	NUM
eurjchem-1252	184	15	,	,	PUNCT
eurjchem-1252	184	16	0.01	0.01	NUM
eurjchem-1252	184	17	)	)	PUNCT
eurjchem-1252	184	18	,	,	PUNCT
eurjchem-1252	184	19	389	389	NUM
eurjchem-1252	184	20	(	(	PUNCT
eurjchem-1252	184	21	0.23	0.23	NUM
eurjchem-1252	184	22	)	)	PUNCT
eurjchem-1252	184	23	,	,	PUNCT
eurjchem-1252	184	24	378	378	NUM
eurjchem-1252	184	25	(	(	PUNCT
eurjchem-1252	184	26	0.07	0.07	NUM
eurjchem-1252	184	27	)	)	PUNCT
eurjchem-1252	184	28	,	,	PUNCT
eurjchem-1252	184	29	335	335	NUM
eurjchem-1252	184	30	(	(	PUNCT
eurjchem-1252	184	31	0.42	0.42	NUM
eurjchem-1252	184	32	)	)	PUNCT
eurjchem-1252	184	33	,	,	PUNCT
eurjchem-1252	184	34	307	307	NUM
eurjchem-1252	184	35	(	(	PUNCT
eurjchem-1252	184	36	0.67	0.67	NUM
eurjchem-1252	184	37	)	)	PUNCT
eurjchem-1252	184	38	,	,	PUNCT
eurjchem-1252	184	39	281	281	NUM
eurjchem-1252	184	40	(	(	PUNCT
eurjchem-1252	184	41	1.02	1.02	NUM
eurjchem-1252	184	42	)	)	PUNCT
eurjchem-1252	184	43	,	,	PUNCT
eurjchem-1252	184	44	277	277	NUM
eurjchem-1252	184	45	(	(	PUNCT
eurjchem-1252	184	46	100	100	NUM
eurjchem-1252	184	47	)	)	PUNCT
eurjchem-1252	184	48	,	,	PUNCT
eurjchem-1252	184	49	267	267	NUM
eurjchem-1252	184	50	(	(	PUNCT
eurjchem-1252	184	51	2.15	2.15	NUM
eurjchem-1252	184	52	)	)	PUNCT
eurjchem-1252	184	53	,	,	PUNCT
eurjchem-1252	184	54	228	228	NUM
eurjchem-1252	184	55	(	(	PUNCT
eurjchem-1252	184	56	1.10	1.10	NUM
eurjchem-1252	184	57	)	)	PUNCT
eurjchem-1252	184	58	,	,	PUNCT
eurjchem-1252	184	59	214	214	NUM
eurjchem-1252	184	60	(	(	PUNCT
eurjchem-1252	184	61	0.32	0.32	NUM
eurjchem-1252	184	62	)	)	PUNCT
eurjchem-1252	184	63	,	,	PUNCT
eurjchem-1252	184	64	206	206	NUM
eurjchem-1252	184	65	(	(	PUNCT
eurjchem-1252	184	66	1.04	1.04	NUM
eurjchem-1252	184	67	)	)	PUNCT
eurjchem-1252	184	68	,	,	PUNCT
eurjchem-1252	184	69	200	200	NUM
eurjchem-1252	184	70	(	(	PUNCT
eurjchem-1252	184	71	2.39	2.39	NUM
eurjchem-1252	184	72	)	)	PUNCT
eurjchem-1252	184	73	,	,	PUNCT
eurjchem-1252	184	74	192	192	NUM
eurjchem-1252	184	75	(	(	PUNCT
eurjchem-1252	184	76	1.10	1.10	NUM
eurjchem-1252	184	77	)	)	PUNCT
eurjchem-1252	184	78	,	,	PUNCT
eurjchem-1252	184	79	178	178	NUM
eurjchem-1252	184	80	(	(	PUNCT
eurjchem-1252	184	81	1.19	1.19	NUM
eurjchem-1252	184	82	)	)	PUNCT
eurjchem-1252	184	83	,	,	PUNCT
eurjchem-1252	184	84	139	139	NUM
eurjchem-1252	184	85	(	(	PUNCT
eurjchem-1252	184	86	2.23	2.23	NUM
eurjchem-1252	184	87	)	)	PUNCT
eurjchem-1252	184	88	,	,	PUNCT
eurjchem-1252	184	89	125	125	NUM
eurjchem-1252	184	90	(	(	PUNCT
eurjchem-1252	184	91	3.61	3.61	NUM
eurjchem-1252	184	92	)	)	PUNCT
eurjchem-1252	184	93	,	,	PUNCT
eurjchem-1252	184	94	99	99	NUM
eurjchem-1252	184	95	(	(	PUNCT
eurjchem-1252	184	96	0.03	0.03	NUM
eurjchem-1252	184	97	)	)	PUNCT
eurjchem-1252	184	98	,	,	PUNCT
eurjchem-1252	184	99	71	71	NUM
eurjchem-1252	184	100	(	(	PUNCT
eurjchem-1252	184	101	0.93	0.93	NUM
eurjchem-1252	184	102	)	)	PUNCT
eurjchem-1252	184	103	.	.	PUNCT
eurjchem-1252	185	1	anal	anal	PROPN
eurjchem-1252	185	2	.	.	PUNCT
eurjchem-1252	185	3	calcd	calcd	NOUN
eurjchem-1252	185	4	.	.	PUNCT
eurjchem-1252	186	1	for	for	ADP
eurjchem-1252	186	2	c25h18n4o2	c25h18n4o2	ADJ
eurjchem-1252	186	3	:	:	PUNCT
eurjchem-1252	186	4	c	c	X
eurjchem-1252	186	5	,	,	PUNCT
eurjchem-1252	186	6	73.88	73.88	NUM
eurjchem-1252	186	7	;	;	PUNCT
eurjchem-1252	186	8	h	h	NOUN
eurjchem-1252	186	9	,	,	PUNCT
eurjchem-1252	186	10	4.46	4.46	NUM
eurjchem-1252	186	11	;	;	PUNCT
eurjchem-1252	186	12	n	n	CCONJ
eurjchem-1252	186	13	,	,	PUNCT
eurjchem-1252	186	14	13.78	13.78	NUM
eurjchem-1252	186	15	.	.	PUNCT
eurjchem-1252	186	16	found	find	VERB
eurjchem-1252	186	17	:	:	PUNCT
eurjchem-1252	187	1	c	c	X
eurjchem-1252	187	2	,	,	PUNCT
eurjchem-1252	187	3	74.17	74.17	NUM
eurjchem-1252	187	4	;	;	PUNCT
eurjchem-1252	187	5	h	h	NOUN
eurjchem-1252	187	6	,	,	PUNCT
eurjchem-1252	187	7	4.38	4.38	NUM
eurjchem-1252	187	8	;	;	PUNCT
eurjchem-1252	187	9	n	n	CCONJ
eurjchem-1252	187	10	,	,	PUNCT
eurjchem-1252	187	11	13.91	13.91	NUM
eurjchem-1252	187	12	%	%	NOUN
eurjchem-1252	187	13	.	.	PUNCT
eurjchem-1252	188	1	method	method	PROPN
eurjchem-1252	188	2	b	b	NOUN
eurjchem-1252	188	3	:	:	PUNCT
eurjchem-1252	188	4	a	a	DET
eurjchem-1252	188	5	solution	solution	NOUN
eurjchem-1252	188	6	of	of	ADP
eurjchem-1252	188	7	compound	compound	NOUN
eurjchem-1252	188	8	10	10	NUM
eurjchem-1252	188	9	(	(	PUNCT
eurjchem-1252	188	10	0.5	0.5	NUM
eurjchem-1252	188	11	g	g	NOUN
eurjchem-1252	188	12	,	,	PUNCT
eurjchem-1252	188	13	1.15	1.15	NUM
eurjchem-1252	188	14	mmol	mmol	NOUN
eurjchem-1252	188	15	)	)	PUNCT
eurjchem-1252	188	16	in	in	ADP
eurjchem-1252	188	17	glacial	glacial	ADJ
eurjchem-1252	188	18	acetic	acetic	ADJ
eurjchem-1252	188	19	acid	acid	NOUN
eurjchem-1252	188	20	(	(	PUNCT
eurjchem-1252	188	21	10	10	NUM
eurjchem-1252	188	22	ml	ml	NOUN
eurjchem-1252	188	23	)	)	PUNCT
eurjchem-1252	188	24	in	in	ADP
eurjchem-1252	188	25	presence	presence	NOUN
eurjchem-1252	188	26	of	of	ADP
eurjchem-1252	188	27	zinc	zinc	NOUN
eurjchem-1252	188	28	dust	dust	NOUN
eurjchem-1252	188	29	was	be	AUX
eurjchem-1252	188	30	refluxed	refluxe	VERB
eurjchem-1252	188	31	for	for	ADP
eurjchem-1252	188	32	2	2	NUM
eurjchem-1252	188	33	h	h	NOUN
eurjchem-1252	188	34	,	,	PUNCT
eurjchem-1252	188	35	then	then	ADV
eurjchem-1252	188	36	filtered	filter	VERB
eurjchem-1252	188	37	on	on	ADP
eurjchem-1252	188	38	hot	hot	ADJ
eurjchem-1252	188	39	.	.	PUNCT
eurjchem-1252	189	1	the	the	DET
eurjchem-1252	189	2	filtrate	filtrate	NOUN
eurjchem-1252	189	3	was	be	AUX
eurjchem-1252	189	4	cooled	cool	VERB
eurjchem-1252	189	5	and	and	CCONJ
eurjchem-1252	189	6	poured	pour	VERB
eurjchem-1252	189	7	into	into	ADP
eurjchem-1252	189	8	water	water	NOUN
eurjchem-1252	189	9	(	(	PUNCT
eurjchem-1252	189	10	100	100	NUM
eurjchem-1252	189	11	ml	ml	NOUN
eurjchem-1252	189	12	)	)	PUNCT
eurjchem-1252	189	13	.	.	PUNCT
eurjchem-1252	190	1	the	the	DET
eurjchem-1252	190	2	precipitate	precipitate	NOUN
eurjchem-1252	190	3	was	be	AUX
eurjchem-1252	190	4	filtered	filter	VERB
eurjchem-1252	190	5	off	off	ADP
eurjchem-1252	190	6	,	,	PUNCT
eurjchem-1252	190	7	washed	wash	VERB
eurjchem-1252	190	8	with	with	ADP
eurjchem-1252	190	9	water	water	NOUN
eurjchem-1252	190	10	,	,	PUNCT
eurjchem-1252	190	11	dried	dry	VERB
eurjchem-1252	190	12	,	,	PUNCT
eurjchem-1252	190	13	and	and	CCONJ
eurjchem-1252	190	14	recrystallized	recrystallize	VERB
eurjchem-1252	190	15	to	to	PART
eurjchem-1252	190	16	give	give	VERB
eurjchem-1252	190	17	compound	compound	NOUN
eurjchem-1252	190	18	9	9	NUM
eurjchem-1252	190	19	.	.	PUNCT
eurjchem-1252	191	1	yield	yield	NOUN
eurjchem-1252	191	2	:	:	PUNCT
eurjchem-1252	191	3	0.26	0.26	NUM
eurjchem-1252	191	4	g	g	NOUN
eurjchem-1252	191	5	,	,	PUNCT
eurjchem-1252	191	6	55.79	55.79	NUM
eurjchem-1252	191	7	%	%	NOUN
eurjchem-1252	191	8	.	.	PUNCT
eurjchem-1252	192	1	2.2.13	2.2.13	NUM
eurjchem-1252	192	2	.	.	PUNCT
eurjchem-1252	193	1	synthesis	synthesis	NOUN
eurjchem-1252	193	2	of	of	ADP
eurjchem-1252	193	3	3‐nitro‐7,8,9‐triphenyl‐2h‐pyrimido	3‐nitro‐7,8,9‐triphenyl‐2h‐pyrimido	NUM
eurjchem-1252	193	4	[	[	X
eurjchem-1252	193	5	1,2‐b]pyridazine‐2,4‐(3h)‐dione	1,2‐b]pyridazine‐2,4‐(3h)‐dione	NUM
eurjchem-1252	193	6	(	(	PUNCT
eurjchem-1252	193	7	10	10	NUM
eurjchem-1252	193	8	)	)	PUNCT
eurjchem-1252	193	9	a	a	DET
eurjchem-1252	193	10	solution	solution	NOUN
eurjchem-1252	193	11	of	of	ADP
eurjchem-1252	193	12	compound	compound	NOUN
eurjchem-1252	193	13	1	1	NUM
eurjchem-1252	193	14	(	(	PUNCT
eurjchem-1252	193	15	0.5	0.5	NUM
eurjchem-1252	193	16	g	g	NOUN
eurjchem-1252	193	17	,	,	PUNCT
eurjchem-1252	193	18	1.28	1.28	NUM
eurjchem-1252	193	19	mmol	mmol	NOUN
eurjchem-1252	193	20	)	)	PUNCT
eurjchem-1252	193	21	in	in	ADP
eurjchem-1252	193	22	glacial	glacial	ADJ
eurjchem-1252	193	23	acetic	acetic	ADJ
eurjchem-1252	193	24	acid	acid	NOUN
eurjchem-1252	193	25	(	(	PUNCT
eurjchem-1252	193	26	5	5	NUM
eurjchem-1252	193	27	ml	ml	NOUN
eurjchem-1252	193	28	)	)	PUNCT
eurjchem-1252	193	29	was	be	AUX
eurjchem-1252	193	30	warmed	warm	VERB
eurjchem-1252	193	31	up	up	ADP
eurjchem-1252	193	32	to	to	ADP
eurjchem-1252	193	33	70	70	NUM
eurjchem-1252	193	34	°	°	ADP
eurjchem-1252	193	35	c	c	NOUN
eurjchem-1252	193	36	with	with	ADP
eurjchem-1252	193	37	stirring	stirring	NOUN
eurjchem-1252	193	38	reacted	react	VERB
eurjchem-1252	193	39	with	with	ADP
eurjchem-1252	193	40	a	a	DET
eurjchem-1252	193	41	mixture	mixture	NOUN
eurjchem-1252	193	42	of	of	ADP
eurjchem-1252	193	43	nano2	nano2	NOUN
eurjchem-1252	193	44	(	(	PUNCT
eurjchem-1252	193	45	0.18	0.18	NUM
eurjchem-1252	193	46	g	g	NOUN
eurjchem-1252	193	47	,	,	PUNCT
eurjchem-1252	193	48	2.56	2.56	NUM
eurjchem-1252	193	49	mmol	mmol	NOUN
eurjchem-1252	193	50	)	)	PUNCT
eurjchem-1252	193	51	,	,	PUNCT
eurjchem-1252	193	52	then	then	ADV
eurjchem-1252	193	53	with	with	ADP
eurjchem-1252	193	54	concentrated	concentrated	ADJ
eurjchem-1252	193	55	nitric	nitric	ADJ
eurjchem-1252	193	56	acid	acid	NOUN
eurjchem-1252	193	57	(	(	PUNCT
eurjchem-1252	193	58	1	1	NUM
eurjchem-1252	193	59	ml	ml	NOUN
eurjchem-1252	193	60	)	)	PUNCT
eurjchem-1252	193	61	.	.	PUNCT
eurjchem-1252	194	1	the	the	DET
eurjchem-1252	194	2	reaction	reaction	NOUN
eurjchem-1252	194	3	mixture	mixture	NOUN
eurjchem-1252	194	4	was	be	AUX
eurjchem-1252	194	5	stirring	stir	VERB
eurjchem-1252	194	6	for	for	ADP
eurjchem-1252	194	7	h.	h.	PROPN
eurjchem-1252	194	8	the	the	DET
eurjchem-1252	194	9	solid	solid	ADJ
eurjchem-1252	194	10	product	product	NOUN
eurjchem-1252	194	11	was	be	AUX
eurjchem-1252	194	12	filtered	filter	VERB
eurjchem-1252	194	13	off	off	ADP
eurjchem-1252	194	14	,	,	PUNCT
eurjchem-1252	194	15	washed	wash	VERB
eurjchem-1252	194	16	with	with	ADP
eurjchem-1252	194	17	water	water	NOUN
eurjchem-1252	194	18	,	,	PUNCT
eurjchem-1252	194	19	dried	dry	VERB
eurjchem-1252	194	20	and	and	CCONJ
eurjchem-1252	194	21	recrystallized	recrystallize	VERB
eurjchem-1252	194	22	from	from	ADP
eurjchem-1252	194	23	ethanol	ethanol	NOUN
eurjchem-1252	194	24	to	to	PART
eurjchem-1252	194	25	give	give	VERB
eurjchem-1252	194	26	compound	compound	NOUN
eurjchem-1252	194	27	10	10	NUM
eurjchem-1252	194	28	(	(	PUNCT
eurjchem-1252	194	29	scheme	scheme	NOUN
eurjchem-1252	194	30	2	2	NUM
eurjchem-1252	194	31	)	)	PUNCT
eurjchem-1252	194	32	.	.	PUNCT
eurjchem-1252	195	1	color	color	NOUN
eurjchem-1252	195	2	:	:	PUNCT
eurjchem-1252	195	3	yellow	yellow	ADJ
eurjchem-1252	195	4	.	.	PUNCT
eurjchem-1252	196	1	yield	yield	NOUN
eurjchem-1252	196	2	:	:	PUNCT
eurjchem-1252	196	3	66.43	66.43	NUM
eurjchem-1252	196	4	%	%	NOUN
eurjchem-1252	196	5	.	.	PUNCT
eurjchem-1252	197	1	m.p	m.p	PROPN
eurjchem-1252	197	2	.	.	PROPN
eurjchem-1252	197	3	:	:	PUNCT
eurjchem-1252	198	1	110‐111	110‐111	PROPN
eurjchem-1252	198	2	°	°	PROPN
eurjchem-1252	198	3	c	c	PROPN
eurjchem-1252	198	4	.	.	PUNCT
eurjchem-1252	199	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	199	2	(	(	PUNCT
eurjchem-1252	199	3	kbr	kbr	PROPN
eurjchem-1252	199	4	,	,	PUNCT
eurjchem-1252	199	5	ν	ν	PROPN
eurjchem-1252	199	6	,	,	PUNCT
eurjchem-1252	199	7	cm‐1	cm‐1	PROPN
eurjchem-1252	199	8	):	):	PUNCT
eurjchem-1252	199	9	3431	3431	NUM
eurjchem-1252	199	10	(	(	PUNCT
eurjchem-1252	199	11	oh	oh	INTJ
eurjchem-1252	199	12	)	)	PUNCT
eurjchem-1252	199	13	,	,	PUNCT
eurjchem-1252	199	14	3057	3057	NUM
eurjchem-1252	199	15	(	(	PUNCT
eurjchem-1252	199	16	ch	ch	NOUN
eurjchem-1252	199	17	,	,	PUNCT
eurjchem-1252	199	18	arom	arom	NOUN
eurjchem-1252	199	19	.	.	PUNCT
eurjchem-1252	199	20	)	)	PUNCT
eurjchem-1252	199	21	,	,	PUNCT
eurjchem-1252	199	22	1721	1721	NUM
eurjchem-1252	199	23	(	(	PUNCT
eurjchem-1252	199	24	c	c	NOUN
eurjchem-1252	199	25	=	=	NOUN
eurjchem-1252	199	26	o	o	NOUN
eurjchem-1252	199	27	)	)	PUNCT
eurjchem-1252	199	28	,	,	PUNCT
eurjchem-1252	199	29	1645	1645	NUM
eurjchem-1252	199	30	(	(	PUNCT
eurjchem-1252	199	31	c	c	NOUN
eurjchem-1252	199	32	=	=	SYM
eurjchem-1252	199	33	n	n	NUM
eurjchem-1252	199	34	)	)	PUNCT
eurjchem-1252	199	35	,	,	PUNCT
eurjchem-1252	199	36	1521	1521	NUM
eurjchem-1252	199	37	(	(	PUNCT
eurjchem-1252	199	38	no2	no2	NOUN
eurjchem-1252	199	39	,	,	PUNCT
eurjchem-1252	199	40	asym	asym	PROPN
eurjchem-1252	199	41	.	.	PROPN
eurjchem-1252	199	42	)	)	PUNCT
eurjchem-1252	199	43	,	,	PUNCT
eurjchem-1252	199	44	1345	1345	NUM
eurjchem-1252	199	45	(	(	PUNCT
eurjchem-1252	199	46	no2	no2	NOUN
eurjchem-1252	199	47	,	,	PUNCT
eurjchem-1252	199	48	sym	sym	NOUN
eurjchem-1252	199	49	.	.	PUNCT
eurjchem-1252	199	50	)	)	PUNCT
eurjchem-1252	199	51	.	.	PUNCT
eurjchem-1252	200	1	ms	ms	NOUN
eurjchem-1252	200	2	(	(	PUNCT
eurjchem-1252	200	3	ei	ei	PROPN
eurjchem-1252	200	4	,	,	PUNCT
eurjchem-1252	200	5	m	m	PROPN
eurjchem-1252	200	6	/	/	SYM
eurjchem-1252	200	7	z	z	PROPN
eurjchem-1252	200	8	(	(	PUNCT
eurjchem-1252	200	9	%	%	NOUN
eurjchem-1252	200	10	)	)	PUNCT
eurjchem-1252	200	11	):	):	PUNCT
eurjchem-1252	200	12	436	436	NUM
eurjchem-1252	200	13	(	(	PUNCT
eurjchem-1252	200	14	m+	m+	NUM
eurjchem-1252	200	15	,	,	PUNCT
eurjchem-1252	200	16	14.91	14.91	NUM
eurjchem-1252	200	17	)	)	PUNCT
eurjchem-1252	200	18	,	,	PUNCT
eurjchem-1252	200	19	419	419	NUM
eurjchem-1252	200	20	(	(	PUNCT
eurjchem-1252	200	21	16.26	16.26	NUM
eurjchem-1252	200	22	)	)	PUNCT
eurjchem-1252	200	23	,	,	PUNCT
eurjchem-1252	200	24	393	393	NUM
eurjchem-1252	200	25	(	(	PUNCT
eurjchem-1252	200	26	14.63	14.63	NUM
eurjchem-1252	200	27	)	)	PUNCT
eurjchem-1252	200	28	,	,	PUNCT
eurjchem-1252	200	29	355	355	NUM
eurjchem-1252	200	30	(	(	PUNCT
eurjchem-1252	200	31	14.09	14.09	NUM
eurjchem-1252	200	32	)	)	PUNCT
eurjchem-1252	200	33	,	,	PUNCT
eurjchem-1252	200	34	333	333	NUM
eurjchem-1252	200	35	(	(	PUNCT
eurjchem-1252	200	36	14.91	14.91	NUM
eurjchem-1252	200	37	)	)	PUNCT
eurjchem-1252	200	38	,	,	PUNCT
eurjchem-1252	200	39	307	307	NUM
eurjchem-1252	200	40	(	(	PUNCT
eurjchem-1252	200	41	14.63	14.63	NUM
eurjchem-1252	200	42	)	)	PUNCT
eurjchem-1252	200	43	,	,	PUNCT
eurjchem-1252	200	44	230	230	NUM
eurjchem-1252	200	45	(	(	PUNCT
eurjchem-1252	200	46	14.09	14.09	NUM
eurjchem-1252	200	47	)	)	PUNCT
eurjchem-1252	200	48	,	,	PUNCT
eurjchem-1252	200	49	206	206	NUM
eurjchem-1252	200	50	(	(	PUNCT
eurjchem-1252	200	51	17.62	17.62	NUM
eurjchem-1252	200	52	)	)	PUNCT
eurjchem-1252	200	53	,	,	PUNCT
eurjchem-1252	200	54	155	155	NUM
eurjchem-1252	200	55	(	(	PUNCT
eurjchem-1252	200	56	19.24	19.24	NUM
eurjchem-1252	200	57	)	)	PUNCT
eurjchem-1252	200	58	,	,	PUNCT
eurjchem-1252	200	59	80	80	NUM
eurjchem-1252	200	60	(	(	PUNCT
eurjchem-1252	200	61	100	100	NUM
eurjchem-1252	200	62	)	)	PUNCT
eurjchem-1252	200	63	.	.	PUNCT
eurjchem-1252	201	1	anal	anal	PROPN
eurjchem-1252	201	2	.	.	PUNCT
eurjchem-1252	201	3	calcd	calcd	NOUN
eurjchem-1252	201	4	.	.	PUNCT
eurjchem-1252	202	1	for	for	ADP
eurjchem-1252	202	2	c25h16n4o4	c25h16n4o4	X
eurjchem-1252	202	3	:	:	PUNCT
eurjchem-1252	202	4	c	c	X
eurjchem-1252	202	5	,	,	PUNCT
eurjchem-1252	202	6	68.80	68.80	NUM
eurjchem-1252	202	7	;	;	PUNCT
eurjchem-1252	202	8	h	h	NOUN
eurjchem-1252	202	9	,	,	PUNCT
eurjchem-1252	202	10	3.70	3.70	NUM
eurjchem-1252	202	11	;	;	PUNCT
eurjchem-1252	202	12	n	n	CCONJ
eurjchem-1252	202	13	,	,	PUNCT
eurjchem-1252	202	14	12.84	12.84	NUM
eurjchem-1252	202	15	.	.	PUNCT
eurjchem-1252	202	16	found	find	VERB
eurjchem-1252	202	17	:	:	PUNCT
eurjchem-1252	203	1	c	c	X
eurjchem-1252	203	2	,	,	PUNCT
eurjchem-1252	203	3	68.55	68.55	NUM
eurjchem-1252	203	4	;	;	PUNCT
eurjchem-1252	203	5	h	h	X
eurjchem-1252	203	6	,	,	PUNCT
eurjchem-1252	203	7	3.87	3.87	NUM
eurjchem-1252	203	8	;	;	PUNCT
eurjchem-1252	203	9	n	n	CCONJ
eurjchem-1252	203	10	,	,	PUNCT
eurjchem-1252	203	11	13.09	13.09	NUM
eurjchem-1252	203	12	%	%	NOUN
eurjchem-1252	203	13	.	.	PUNCT
eurjchem-1252	204	1	2.2.14	2.2.14	X
eurjchem-1252	204	2	.	.	PUNCT
eurjchem-1252	205	1	synthesis	synthesis	NOUN
eurjchem-1252	205	2	of	of	ADP
eurjchem-1252	205	3	2‐chloro‐3‐nitro‐7,8,9‐triphenyl‐4h‐	2‐chloro‐3‐nitro‐7,8,9‐triphenyl‐4h‐	NUM
eurjchem-1252	205	4	pyrimido[1,2‐b]pyridazin‐4‐one	pyrimido[1,2‐b]pyridazin‐4‐one	NOUN
eurjchem-1252	205	5	(	(	PUNCT
eurjchem-1252	205	6	11	11	NUM
eurjchem-1252	205	7	)	)	PUNCT
eurjchem-1252	205	8	a	a	DET
eurjchem-1252	205	9	mixture	mixture	NOUN
eurjchem-1252	205	10	of	of	ADP
eurjchem-1252	205	11	compound	compound	NOUN
eurjchem-1252	205	12	10	10	NUM
eurjchem-1252	205	13	(	(	PUNCT
eurjchem-1252	205	14	0.5	0.5	NUM
eurjchem-1252	205	15	g	g	NOUN
eurjchem-1252	205	16	,	,	PUNCT
eurjchem-1252	205	17	1.15	1.15	NUM
eurjchem-1252	205	18	mmol	mmol	NOUN
eurjchem-1252	205	19	)	)	PUNCT
eurjchem-1252	205	20	and	and	CCONJ
eurjchem-1252	205	21	phosphoryl	phosphoryl	PROPN
eurjchem-1252	205	22	chloride	chloride	PROPN
eurjchem-1252	205	23	(	(	PUNCT
eurjchem-1252	205	24	10	10	NUM
eurjchem-1252	205	25	ml	ml	NOUN
eurjchem-1252	205	26	)	)	PUNCT
eurjchem-1252	205	27	was	be	AUX
eurjchem-1252	205	28	refluxed	refluxe	VERB
eurjchem-1252	205	29	for	for	ADP
eurjchem-1252	205	30	3	3	NUM
eurjchem-1252	205	31	h.	h.	NOUN
eurjchem-1252	205	32	the	the	DET
eurjchem-1252	205	33	reaction	reaction	NOUN
eurjchem-1252	205	34	mixture	mixture	NOUN
eurjchem-1252	205	35	was	be	AUX
eurjchem-1252	205	36	cooled	cool	VERB
eurjchem-1252	205	37	,	,	PUNCT
eurjchem-1252	205	38	and	and	CCONJ
eurjchem-1252	205	39	poured	pour	VERB
eurjchem-1252	205	40	into	into	ADP
eurjchem-1252	205	41	ice	ice	NOUN
eurjchem-1252	205	42	water	water	NOUN
eurjchem-1252	205	43	(	(	PUNCT
eurjchem-1252	205	44	200	200	NUM
eurjchem-1252	205	45	ml	ml	NOUN
eurjchem-1252	205	46	)	)	PUNCT
eurjchem-1252	205	47	.	.	PUNCT
eurjchem-1252	206	1	the	the	DET
eurjchem-1252	206	2	solid	solid	ADJ
eurjchem-1252	206	3	product	product	NOUN
eurjchem-1252	206	4	was	be	AUX
eurjchem-1252	206	5	filtered	filter	VERB
eurjchem-1252	206	6	off	off	ADP
eurjchem-1252	206	7	,	,	PUNCT
eurjchem-1252	206	8	washed	wash	VERB
eurjchem-1252	206	9	with	with	ADP
eurjchem-1252	206	10	water	water	NOUN
eurjchem-1252	206	11	,	,	PUNCT
eurjchem-1252	206	12	dried	dry	VERB
eurjchem-1252	206	13	,	,	PUNCT
eurjchem-1252	206	14	and	and	CCONJ
eurjchem-1252	206	15	recrystallized	recrystallize	VERB
eurjchem-1252	206	16	from	from	ADP
eurjchem-1252	206	17	ethanol	ethanol	NOUN
eurjchem-1252	206	18	to	to	PART
eurjchem-1252	206	19	give	give	VERB
eurjchem-1252	206	20	compound	compound	NOUN
eurjchem-1252	206	21	11	11	NUM
eurjchem-1252	206	22	(	(	PUNCT
eurjchem-1252	206	23	scheme	scheme	NOUN
eurjchem-1252	206	24	2	2	NUM
eurjchem-1252	206	25	)	)	PUNCT
eurjchem-1252	206	26	.	.	PUNCT
eurjchem-1252	207	1	color	color	NOUN
eurjchem-1252	207	2	:	:	PUNCT
eurjchem-1252	207	3	brown	brown	ADJ
eurjchem-1252	207	4	.	.	PUNCT
eurjchem-1252	208	1	yield	yield	NOUN
eurjchem-1252	208	2	:	:	PUNCT
eurjchem-1252	208	3	69.10	69.10	NUM
eurjchem-1252	208	4	%	%	NOUN
eurjchem-1252	208	5	.	.	PUNCT
eurjchem-1252	209	1	m.p	m.p	PROPN
eurjchem-1252	209	2	.	.	PROPN
eurjchem-1252	209	3	:	:	PUNCT
eurjchem-1252	210	1	152‐154	152‐154	NUM
eurjchem-1252	210	2	°	°	ADP
eurjchem-1252	210	3	c	c	NOUN
eurjchem-1252	210	4	.	.	PUNCT
eurjchem-1252	211	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	211	2	(	(	PUNCT
eurjchem-1252	211	3	kbr	kbr	PROPN
eurjchem-1252	211	4	,	,	PUNCT
eurjchem-1252	211	5	ν	ν	PROPN
eurjchem-1252	211	6	,	,	PUNCT
eurjchem-1252	211	7	cm‐1	cm‐1	PROPN
eurjchem-1252	211	8	):	):	PUNCT
eurjchem-1252	211	9	3057	3057	NUM
eurjchem-1252	211	10	(	(	PUNCT
eurjchem-1252	211	11	ch	ch	NOUN
eurjchem-1252	211	12	,	,	PUNCT
eurjchem-1252	211	13	arom	arom	NOUN
eurjchem-1252	211	14	.	.	PUNCT
eurjchem-1252	211	15	)	)	PUNCT
eurjchem-1252	211	16	,	,	PUNCT
eurjchem-1252	211	17	1718	1718	NUM
eurjchem-1252	211	18	(	(	PUNCT
eurjchem-1252	211	19	c	c	NOUN
eurjchem-1252	211	20	=	=	NOUN
eurjchem-1252	211	21	o	o	NOUN
eurjchem-1252	211	22	)	)	PUNCT
eurjchem-1252	211	23	,	,	PUNCT
eurjchem-1252	211	24	1640	1640	NUM
eurjchem-1252	211	25	(	(	PUNCT
eurjchem-1252	211	26	c	c	NOUN
eurjchem-1252	211	27	=	=	SYM
eurjchem-1252	211	28	n	n	NUM
eurjchem-1252	211	29	)	)	PUNCT
eurjchem-1252	211	30	,	,	PUNCT
eurjchem-1252	211	31	1524	1524	NUM
eurjchem-1252	211	32	(	(	PUNCT
eurjchem-1252	211	33	no2	no2	NOUN
eurjchem-1252	211	34	,	,	PUNCT
eurjchem-1252	211	35	asym	asym	PROPN
eurjchem-1252	211	36	.	.	PROPN
eurjchem-1252	211	37	)	)	PUNCT
eurjchem-1252	211	38	,	,	PUNCT
eurjchem-1252	211	39	1345	1345	NUM
eurjchem-1252	211	40	(	(	PUNCT
eurjchem-1252	211	41	no2	no2	NOUN
eurjchem-1252	211	42	,	,	PUNCT
eurjchem-1252	211	43	sym	sym	NOUN
eurjchem-1252	211	44	.	.	PROPN
eurjchem-1252	211	45	)	)	PUNCT
eurjchem-1252	211	46	.	.	PUNCT
eurjchem-1252	212	1	1h	1h	NUM
eurjchem-1252	212	2	nmr	nmr	NOUN
eurjchem-1252	212	3	(	(	PUNCT
eurjchem-1252	212	4	300	300	NUM
eurjchem-1252	212	5	mhz	mhz	NOUN
eurjchem-1252	212	6	,	,	PUNCT
eurjchem-1252	212	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1252	212	8	,	,	PUNCT
eurjchem-1252	212	9	δ	δ	PROPN
eurjchem-1252	212	10	,	,	PUNCT
eurjchem-1252	212	11	ppm	ppm	NUM
eurjchem-1252	212	12	):	):	PUNCT
eurjchem-1252	212	13	6.94‐7.66	6.94‐7.66	NUM
eurjchem-1252	212	14	(	(	PUNCT
eurjchem-1252	212	15	m	m	PROPN
eurjchem-1252	212	16	,	,	PUNCT
eurjchem-1252	212	17	15h	15h	NUM
eurjchem-1252	212	18	,	,	PUNCT
eurjchem-1252	212	19	3ph	3ph	NOUN
eurjchem-1252	212	20	)	)	PUNCT
eurjchem-1252	212	21	.	.	PUNCT
eurjchem-1252	213	1	ms	ms	NOUN
eurjchem-1252	213	2	(	(	PUNCT
eurjchem-1252	213	3	ei	ei	PROPN
eurjchem-1252	213	4	,	,	PUNCT
eurjchem-1252	213	5	m	m	PROPN
eurjchem-1252	213	6	/	/	SYM
eurjchem-1252	213	7	z	z	PROPN
eurjchem-1252	213	8	(	(	PUNCT
eurjchem-1252	213	9	%	%	NOUN
eurjchem-1252	213	10	)	)	PUNCT
eurjchem-1252	213	11	):	):	PUNCT
eurjchem-1252	213	12	455	455	NUM
eurjchem-1252	213	13	(	(	PUNCT
eurjchem-1252	213	14	m+	m+	NUM
eurjchem-1252	213	15	,	,	PUNCT
eurjchem-1252	213	16	0.54	0.54	NUM
eurjchem-1252	213	17	)	)	PUNCT
eurjchem-1252	213	18	,	,	PUNCT
eurjchem-1252	213	19	409	409	NUM
eurjchem-1252	213	20	(	(	PUNCT
eurjchem-1252	213	21	0.33	0.33	NUM
eurjchem-1252	213	22	)	)	PUNCT
eurjchem-1252	213	23	,	,	PUNCT
eurjchem-1252	213	24	393	393	NUM
eurjchem-1252	213	25	(	(	PUNCT
eurjchem-1252	213	26	1.95	1.95	NUM
eurjchem-1252	213	27	)	)	PUNCT
eurjchem-1252	213	28	,	,	PUNCT
eurjchem-1252	213	29	378	378	NUM
eurjchem-1252	213	30	(	(	PUNCT
eurjchem-1252	213	31	0.33	0.33	NUM
eurjchem-1252	213	32	)	)	PUNCT
eurjchem-1252	213	33	,	,	PUNCT
eurjchem-1252	213	34	281	281	NUM
eurjchem-1252	213	35	(	(	PUNCT
eurjchem-1252	213	36	0.87	0.87	NUM
eurjchem-1252	213	37	)	)	PUNCT
eurjchem-1252	213	38	,	,	PUNCT
eurjchem-1252	213	39	277	277	NUM
eurjchem-1252	213	40	(	(	PUNCT
eurjchem-1252	213	41	1.63	1.63	NUM
eurjchem-1252	213	42	)	)	PUNCT
eurjchem-1252	213	43	,	,	PUNCT
eurjchem-1252	213	44	267	267	NUM
eurjchem-1252	213	45	(	(	PUNCT
eurjchem-1252	213	46	1.41	1.41	NUM
eurjchem-1252	213	47	)	)	PUNCT
eurjchem-1252	213	48	,	,	PUNCT
eurjchem-1252	213	49	249	249	NUM
eurjchem-1252	213	50	(	(	PUNCT
eurjchem-1252	213	51	0.43	0.43	NUM
eurjchem-1252	213	52	)	)	PUNCT
eurjchem-1252	213	53	,	,	PUNCT
eurjchem-1252	213	54	206	206	NUM
eurjchem-1252	213	55	(	(	PUNCT
eurjchem-1252	213	56	2.28	2.28	NUM
eurjchem-1252	213	57	)	)	PUNCT
eurjchem-1252	213	58	,	,	PUNCT
eurjchem-1252	213	59	188	188	NUM
eurjchem-1252	213	60	(	(	PUNCT
eurjchem-1252	213	61	0.54	0.54	NUM
eurjchem-1252	213	62	)	)	PUNCT
eurjchem-1252	213	63	,	,	PUNCT
eurjchem-1252	213	64	178	178	NUM
eurjchem-1252	213	65	(	(	PUNCT
eurjchem-1252	213	66	5.85	5.85	NUM
eurjchem-1252	213	67	)	)	PUNCT
eurjchem-1252	213	68	,	,	PUNCT
eurjchem-1252	213	69	174	174	NUM
eurjchem-1252	213	70	(	(	PUNCT
eurjchem-1252	213	71	0.87	0.87	NUM
eurjchem-1252	213	72	)	)	PUNCT
eurjchem-1252	213	73	,	,	PUNCT
eurjchem-1252	213	74	77(72.48	77(72.48	NUM
eurjchem-1252	213	75	)	)	PUNCT
eurjchem-1252	213	76	,	,	PUNCT
eurjchem-1252	213	77	62	62	NUM
eurjchem-1252	213	78	(	(	PUNCT
eurjchem-1252	213	79	6.50	6.50	NUM
eurjchem-1252	213	80	)	)	PUNCT
eurjchem-1252	213	81	,	,	PUNCT
eurjchem-1252	213	82	56	56	NUM
eurjchem-1252	213	83	(	(	PUNCT
eurjchem-1252	213	84	100	100	NUM
eurjchem-1252	213	85	)	)	PUNCT
eurjchem-1252	213	86	.	.	PUNCT
eurjchem-1252	214	1	anal	anal	PROPN
eurjchem-1252	214	2	.	.	PUNCT
eurjchem-1252	214	3	calcd	calcd	NOUN
eurjchem-1252	214	4	.	.	PUNCT
eurjchem-1252	215	1	for	for	ADP
eurjchem-1252	215	2	c25h15cln4o3	c25h15cln4o3	NOUN
eurjchem-1252	215	3	:	:	PUNCT
eurjchem-1252	215	4	c	c	X
eurjchem-1252	215	5	,	,	PUNCT
eurjchem-1252	215	6	66.01	66.01	NUM
eurjchem-1252	215	7	;	;	PUNCT
eurjchem-1252	215	8	h	h	NOUN
eurjchem-1252	215	9	,	,	PUNCT
eurjchem-1252	215	10	3.32	3.32	NUM
eurjchem-1252	215	11	;	;	PUNCT
eurjchem-1252	215	12	n	n	CCONJ
eurjchem-1252	215	13	,	,	PUNCT
eurjchem-1252	215	14	12.32	12.32	NUM
eurjchem-1252	215	15	.	.	PUNCT
eurjchem-1252	215	16	found	find	VERB
eurjchem-1252	215	17	:	:	PUNCT
eurjchem-1252	216	1	c	c	X
eurjchem-1252	216	2	,	,	PUNCT
eurjchem-1252	216	3	66.27	66.27	NUM
eurjchem-1252	216	4	;	;	PUNCT
eurjchem-1252	216	5	h	h	NOUN
eurjchem-1252	216	6	,	,	PUNCT
eurjchem-1252	216	7	3.46	3.46	NUM
eurjchem-1252	216	8	;	;	PUNCT
eurjchem-1252	216	9	n	n	CCONJ
eurjchem-1252	216	10	,	,	PUNCT
eurjchem-1252	216	11	12.09	12.09	NUM
eurjchem-1252	216	12	%	%	NOUN
eurjchem-1252	216	13	.	.	PUNCT
eurjchem-1252	217	1	2.2.15	2.2.15	X
eurjchem-1252	217	2	.	.	PUNCT
eurjchem-1252	217	3	synthesis	synthesis	NOUN
eurjchem-1252	217	4	of	of	ADP
eurjchem-1252	217	5	3‐(1‐hydroxyethylidene)‐7,8,9‐	3‐(1‐hydroxyethylidene)‐7,8,9‐	NUM
eurjchem-1252	217	6	triphenyl‐2h‐pyrimido[1,2‐b]pyridazine‐2,4(3h)‐dione	triphenyl‐2h‐pyrimido[1,2‐b]pyridazine‐2,4(3h)‐dione	NOUN
eurjchem-1252	217	7	(	(	PUNCT
eurjchem-1252	217	8	12	12	NUM
eurjchem-1252	217	9	)	)	PUNCT
eurjchem-1252	217	10	a	a	DET
eurjchem-1252	217	11	solution	solution	NOUN
eurjchem-1252	217	12	of	of	ADP
eurjchem-1252	217	13	compound	compound	NOUN
eurjchem-1252	217	14	1	1	NUM
eurjchem-1252	217	15	(	(	PUNCT
eurjchem-1252	217	16	0.5	0.5	NUM
eurjchem-1252	217	17	g	g	NOUN
eurjchem-1252	217	18	,	,	PUNCT
eurjchem-1252	217	19	1.28	1.28	NUM
eurjchem-1252	217	20	mmol	mmol	NOUN
eurjchem-1252	217	21	)	)	PUNCT
eurjchem-1252	217	22	in	in	ADP
eurjchem-1252	217	23	glacial	glacial	ADJ
eurjchem-1252	217	24	acetic	acetic	ADJ
eurjchem-1252	217	25	acid	acid	NOUN
eurjchem-1252	217	26	(	(	PUNCT
eurjchem-1252	217	27	10	10	NUM
eurjchem-1252	217	28	ml	ml	NOUN
eurjchem-1252	217	29	)	)	PUNCT
eurjchem-1252	217	30	in	in	ADP
eurjchem-1252	217	31	presence	presence	NOUN
eurjchem-1252	217	32	of	of	ADP
eurjchem-1252	217	33	an	an	DET
eurjchem-1252	217	34	excess	excess	ADJ
eurjchem-1252	217	35	polyphosphoric	polyphosphoric	NOUN
eurjchem-1252	217	36	(	(	PUNCT
eurjchem-1252	217	37	1.0	1.0	NUM
eurjchem-1252	217	38	g	g	NOUN
eurjchem-1252	217	39	)	)	PUNCT
eurjchem-1252	217	40	acid	acid	NOUN
eurjchem-1252	217	41	was	be	AUX
eurjchem-1252	217	42	refluxed	refluxe	VERB
eurjchem-1252	217	43	for	for	ADP
eurjchem-1252	217	44	2	2	NUM
eurjchem-1252	217	45	h.	h.	NOUN
eurjchem-1252	217	46	the	the	DET
eurjchem-1252	217	47	reaction	reaction	NOUN
eurjchem-1252	217	48	mixture	mixture	NOUN
eurjchem-1252	217	49	was	be	AUX
eurjchem-1252	217	50	cooled	cool	VERB
eurjchem-1252	217	51	,	,	PUNCT
eurjchem-1252	217	52	poured	pour	VERB
eurjchem-1252	217	53	into	into	ADP
eurjchem-1252	217	54	ice	ice	NOUN
eurjchem-1252	217	55	cold	cold	ADJ
eurjchem-1252	217	56	water	water	NOUN
eurjchem-1252	217	57	(	(	PUNCT
eurjchem-1252	217	58	200	200	NUM
eurjchem-1252	217	59	ml	ml	NOUN
eurjchem-1252	217	60	)	)	PUNCT
eurjchem-1252	217	61	,	,	PUNCT
eurjchem-1252	217	62	and	and	CCONJ
eurjchem-1252	217	63	then	then	ADV
eurjchem-1252	217	64	the	the	DET
eurjchem-1252	217	65	solid	solid	ADJ
eurjchem-1252	217	66	product	product	NOUN
eurjchem-1252	217	67	formed	form	VERB
eurjchem-1252	217	68	was	be	AUX
eurjchem-1252	217	69	filtered	filter	VERB
eurjchem-1252	217	70	off	off	ADP
eurjchem-1252	217	71	,	,	PUNCT
eurjchem-1252	217	72	washed	wash	VERB
eurjchem-1252	217	73	with	with	ADP
eurjchem-1252	217	74	water	water	NOUN
eurjchem-1252	217	75	,	,	PUNCT
eurjchem-1252	217	76	dried	dry	VERB
eurjchem-1252	217	77	,	,	PUNCT
eurjchem-1252	217	78	and	and	CCONJ
eurjchem-1252	217	79	recrystallized	recrystallize	VERB
eurjchem-1252	217	80	from	from	ADP
eurjchem-1252	217	81	acetone	acetone	NOUN
eurjchem-1252	217	82	to	to	PART
eurjchem-1252	217	83	give	give	VERB
eurjchem-1252	217	84	compound	compound	NOUN
eurjchem-1252	217	85	12	12	NUM
eurjchem-1252	217	86	(	(	PUNCT
eurjchem-1252	217	87	scheme	scheme	NOUN
eurjchem-1252	217	88	3	3	NUM
eurjchem-1252	217	89	)	)	PUNCT
eurjchem-1252	217	90	.	.	PUNCT
eurjchem-1252	218	1	color	color	NOUN
eurjchem-1252	218	2	:	:	PUNCT
eurjchem-1252	218	3	yellow	yellow	ADJ
eurjchem-1252	218	4	.	.	PUNCT
eurjchem-1252	219	1	yield	yield	NOUN
eurjchem-1252	219	2	:	:	PUNCT
eurjchem-1252	219	3	70.43	70.43	NUM
eurjchem-1252	219	4	%	%	NOUN
eurjchem-1252	219	5	.	.	PUNCT
eurjchem-1252	220	1	m.p	m.p	PROPN
eurjchem-1252	220	2	.	.	PROPN
eurjchem-1252	220	3	:	:	PUNCT
eurjchem-1252	221	1	214‐215	214‐215	NUM
eurjchem-1252	221	2	°	°	PRON
eurjchem-1252	221	3	c	c	NOUN
eurjchem-1252	221	4	.	.	PUNCT
eurjchem-1252	222	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	222	2	(	(	PUNCT
eurjchem-1252	222	3	kbr	kbr	PROPN
eurjchem-1252	222	4	,	,	PUNCT
eurjchem-1252	222	5	ν	ν	PROPN
eurjchem-1252	222	6	,	,	PUNCT
eurjchem-1252	222	7	cm‐1	cm‐1	PROPN
eurjchem-1252	222	8	):	):	PUNCT
eurjchem-1252	222	9	3056	3056	NUM
eurjchem-1252	222	10	(	(	PUNCT
eurjchem-1252	222	11	ch	ch	NOUN
eurjchem-1252	222	12	,	,	PUNCT
eurjchem-1252	222	13	arom	arom	NOUN
eurjchem-1252	222	14	.	.	PUNCT
eurjchem-1252	222	15	)	)	PUNCT
eurjchem-1252	222	16	,	,	PUNCT
eurjchem-1252	222	17	2921	2921	NUM
eurjchem-1252	222	18	,	,	PUNCT
eurjchem-1252	222	19	2851	2851	NUM
eurjchem-1252	222	20	(	(	PUNCT
eurjchem-1252	222	21	ch	ch	NOUN
eurjchem-1252	222	22	,	,	PUNCT
eurjchem-1252	222	23	aliph	aliph	NOUN
eurjchem-1252	222	24	.	.	PUNCT
eurjchem-1252	222	25	)	)	PUNCT
eurjchem-1252	222	26	,	,	PUNCT
eurjchem-1252	222	27	1713	1713	NUM
eurjchem-1252	222	28	(	(	PUNCT
eurjchem-1252	222	29	c	c	NOUN
eurjchem-1252	222	30	=	=	NOUN
eurjchem-1252	222	31	o	o	NOUN
eurjchem-1252	222	32	)	)	PUNCT
eurjchem-1252	222	33	,	,	PUNCT
eurjchem-1252	222	34	1647	1647	NUM
eurjchem-1252	222	35	(	(	PUNCT
eurjchem-1252	222	36	c	c	NOUN
eurjchem-1252	222	37	=	=	SYM
eurjchem-1252	222	38	n	n	NUM
eurjchem-1252	222	39	)	)	PUNCT
eurjchem-1252	222	40	.	.	PUNCT
eurjchem-1252	223	1	ms	ms	NOUN
eurjchem-1252	223	2	(	(	PUNCT
eurjchem-1252	223	3	ei	ei	PROPN
eurjchem-1252	223	4	,	,	PUNCT
eurjchem-1252	223	5	m	m	PROPN
eurjchem-1252	223	6	/	/	SYM
eurjchem-1252	223	7	z	z	PROPN
eurjchem-1252	223	8	(	(	PUNCT
eurjchem-1252	223	9	%	%	NOUN
eurjchem-1252	223	10	)	)	PUNCT
eurjchem-1252	223	11	):	):	PUNCT
eurjchem-1252	223	12	433	433	NUM
eurjchem-1252	223	13	(	(	PUNCT
eurjchem-1252	223	14	m+	m+	NUM
eurjchem-1252	223	15	,	,	PUNCT
eurjchem-1252	223	16	70.87	70.87	NUM
eurjchem-1252	223	17	)	)	PUNCT
eurjchem-1252	223	18	,	,	PUNCT
eurjchem-1252	223	19	415	415	NUM
eurjchem-1252	223	20	(	(	PUNCT
eurjchem-1252	223	21	61.71	61.71	NUM
eurjchem-1252	223	22	)	)	PUNCT
eurjchem-1252	223	23	,	,	PUNCT
eurjchem-1252	223	24	390	390	NUM
eurjchem-1252	223	25	(	(	PUNCT
eurjchem-1252	223	26	58.25	58.25	NUM
eurjchem-1252	223	27	)	)	PUNCT
eurjchem-1252	223	28	,	,	PUNCT
eurjchem-1252	223	29	348	348	NUM
eurjchem-1252	223	30	(	(	PUNCT
eurjchem-1252	223	31	61.17	61.17	NUM
eurjchem-1252	223	32	)	)	PUNCT
eurjchem-1252	223	33	,	,	PUNCT
eurjchem-1252	223	34	326	326	NUM
eurjchem-1252	223	35	(	(	PUNCT
eurjchem-1252	223	36	100	100	NUM
eurjchem-1252	223	37	)	)	PUNCT
eurjchem-1252	223	38	,	,	PUNCT
eurjchem-1252	223	39	319	319	NUM
eurjchem-1252	223	40	(	(	PUNCT
eurjchem-1252	223	41	76.70	76.70	NUM
eurjchem-1252	223	42	)	)	PUNCT
eurjchem-1252	223	43	,	,	PUNCT
eurjchem-1252	223	44	307	307	NUM
eurjchem-1252	223	45	(	(	PUNCT
eurjchem-1252	223	46	73.79	73.79	NUM
eurjchem-1252	223	47	)	)	PUNCT
eurjchem-1252	223	48	,	,	PUNCT
eurjchem-1252	223	49	279	279	NUM
eurjchem-1252	223	50	(	(	PUNCT
eurjchem-1252	223	51	53.40	53.40	NUM
eurjchem-1252	223	52	)	)	PUNCT
eurjchem-1252	223	53	,	,	PUNCT
eurjchem-1252	223	54	152	152	NUM
eurjchem-1252	223	55	(	(	PUNCT
eurjchem-1252	223	56	52.43	52.43	NUM
eurjchem-1252	223	57	)	)	PUNCT
eurjchem-1252	223	58	,	,	PUNCT
eurjchem-1252	223	59	126	126	NUM
eurjchem-1252	223	60	(	(	PUNCT
eurjchem-1252	223	61	64.08	64.08	NUM
eurjchem-1252	223	62	)	)	PUNCT
eurjchem-1252	223	63	,	,	PUNCT
eurjchem-1252	223	64	109	109	NUM
eurjchem-1252	223	65	(	(	PUNCT
eurjchem-1252	223	66	89.32	89.32	NUM
eurjchem-1252	223	67	)	)	PUNCT
eurjchem-1252	223	68	,	,	PUNCT
eurjchem-1252	223	69	83	83	NUM
eurjchem-1252	223	70	(	(	PUNCT
eurjchem-1252	223	71	18.45	18.45	NUM
eurjchem-1252	223	72	)	)	PUNCT
eurjchem-1252	223	73	,	,	PUNCT
eurjchem-1252	223	74	79	79	NUM
eurjchem-1252	223	75	(	(	PUNCT
eurjchem-1252	223	76	83.50	83.50	NUM
eurjchem-1252	223	77	)	)	PUNCT
eurjchem-1252	223	78	,	,	PUNCT
eurjchem-1252	223	79	76	76	NUM
eurjchem-1252	223	80	(	(	PUNCT
eurjchem-1252	223	81	67.96	67.96	NUM
eurjchem-1252	223	82	)	)	PUNCT
eurjchem-1252	223	83	.	.	PUNCT
eurjchem-1252	224	1	anal	anal	PROPN
eurjchem-1252	224	2	.	.	PUNCT
eurjchem-1252	224	3	calcd	calcd	NOUN
eurjchem-1252	224	4	.	.	PUNCT
eurjchem-1252	225	1	for	for	ADP
eurjchem-1252	225	2	c27h19n3o3	c27h19n3o3	PROPN
eurjchem-1252	225	3	:	:	PUNCT
eurjchem-1252	225	4	c	c	X
eurjchem-1252	225	5	,	,	PUNCT
eurjchem-1252	225	6	74.81	74.81	NUM
eurjchem-1252	225	7	;	;	PUNCT
eurjchem-1252	225	8	h	h	NOUN
eurjchem-1252	225	9	,	,	PUNCT
eurjchem-1252	225	10	4.42	4.42	NUM
eurjchem-1252	225	11	;	;	PUNCT
eurjchem-1252	225	12	n	n	CCONJ
eurjchem-1252	225	13	,	,	PUNCT
eurjchem-1252	225	14	9.69	9.69	NUM
eurjchem-1252	225	15	.	.	PUNCT
eurjchem-1252	225	16	found	find	VERB
eurjchem-1252	225	17	:	:	PUNCT
eurjchem-1252	226	1	c	c	X
eurjchem-1252	226	2	,	,	PUNCT
eurjchem-1252	226	3	75.13	75.13	NUM
eurjchem-1252	226	4	;	;	PUNCT
eurjchem-1252	226	5	h	h	NOUN
eurjchem-1252	226	6	,	,	PUNCT
eurjchem-1252	226	7	4.58	4.58	NUM
eurjchem-1252	226	8	;	;	PUNCT
eurjchem-1252	226	9	n	n	CCONJ
eurjchem-1252	226	10	,	,	PUNCT
eurjchem-1252	226	11	9.87	9.87	NUM
eurjchem-1252	226	12	%	%	NOUN
eurjchem-1252	226	13	.	.	PUNCT
eurjchem-1252	227	1	2.2.16	2.2.16	NUM
eurjchem-1252	227	2	.	.	PUNCT
eurjchem-1252	228	1	synthesis	synthesis	NOUN
eurjchem-1252	228	2	of	of	ADP
eurjchem-1252	228	3	3‐(1‐hydroxy‐3‐phenylallylidene)‐7,8,9‐	3‐(1‐hydroxy‐3‐phenylallylidene)‐7,8,9‐	NUM
eurjchem-1252	228	4	triphenyl‐2h‐pyrimido[1,2‐b]pyridazine‐2,4(3h)‐dione	triphenyl‐2h‐pyrimido[1,2‐b]pyridazine‐2,4(3h)‐dione	NOUN
eurjchem-1252	228	5	(	(	PUNCT
eurjchem-1252	228	6	13	13	NUM
eurjchem-1252	228	7	)	)	PUNCT
eurjchem-1252	228	8	a	a	DET
eurjchem-1252	228	9	solution	solution	NOUN
eurjchem-1252	228	10	of	of	ADP
eurjchem-1252	228	11	compound	compound	NOUN
eurjchem-1252	228	12	12	12	NUM
eurjchem-1252	228	13	(	(	PUNCT
eurjchem-1252	228	14	0.5	0.5	NUM
eurjchem-1252	228	15	g	g	NOUN
eurjchem-1252	228	16	,	,	PUNCT
eurjchem-1252	228	17	1.15	1.15	NUM
eurjchem-1252	228	18	mmol	mmol	NOUN
eurjchem-1252	228	19	)	)	PUNCT
eurjchem-1252	228	20	and	and	CCONJ
eurjchem-1252	228	21	benzaldehyde	benzaldehyde	NOUN
eurjchem-1252	228	22	(	(	PUNCT
eurjchem-1252	228	23	0.12	0.12	NUM
eurjchem-1252	228	24	ml	ml	NOUN
eurjchem-1252	228	25	,	,	PUNCT
eurjchem-1252	228	26	1.15	1.15	NUM
eurjchem-1252	228	27	mmol	mmol	NOUN
eurjchem-1252	228	28	)	)	PUNCT
eurjchem-1252	228	29	in	in	ADP
eurjchem-1252	228	30	ethanol	ethanol	NOUN
eurjchem-1252	228	31	(	(	PUNCT
eurjchem-1252	228	32	10	10	NUM
eurjchem-1252	228	33	ml	ml	NOUN
eurjchem-1252	228	34	)	)	PUNCT
eurjchem-1252	228	35	in	in	ADP
eurjchem-1252	228	36	presence	presence	NOUN
eurjchem-1252	228	37	of	of	ADP
eurjchem-1252	228	38	sodium	sodium	NOUN
eurjchem-1252	228	39	hydroxide	hydroxide	NOUN
eurjchem-1252	228	40	(	(	PUNCT
eurjchem-1252	228	41	0.1	0.1	NUM
eurjchem-1252	228	42	g	g	NOUN
eurjchem-1252	228	43	)	)	PUNCT
eurjchem-1252	228	44	was	be	AUX
eurjchem-1252	228	45	stirred	stir	VERB
eurjchem-1252	228	46	at	at	ADP
eurjchem-1252	228	47	room	room	NOUN
eurjchem-1252	228	48	temperature	temperature	NOUN
eurjchem-1252	228	49	for	for	ADP
eurjchem-1252	228	50	1	1	NUM
eurjchem-1252	228	51	h.	h.	NOUN
eurjchem-1252	228	52	the	the	DET
eurjchem-1252	228	53	solid	solid	ADJ
eurjchem-1252	228	54	product	product	NOUN
eurjchem-1252	228	55	formed	form	VERB
eurjchem-1252	228	56	was	be	AUX
eurjchem-1252	228	57	collected	collect	VERB
eurjchem-1252	228	58	,	,	PUNCT
eurjchem-1252	228	59	washed	wash	VERB
eurjchem-1252	228	60	with	with	ADP
eurjchem-1252	228	61	water	water	NOUN
eurjchem-1252	228	62	,	,	PUNCT
eurjchem-1252	228	63	dried	dry	VERB
eurjchem-1252	228	64	,	,	PUNCT
eurjchem-1252	228	65	and	and	CCONJ
eurjchem-1252	228	66	recrystallized	recrystallize	VERB
eurjchem-1252	228	67	from	from	ADP
eurjchem-1252	228	68	ethanol	ethanol	NOUN
eurjchem-1252	228	69	to	to	PART
eurjchem-1252	228	70	give	give	VERB
eurjchem-1252	228	71	compound	compound	NOUN
eurjchem-1252	228	72	13	13	NUM
eurjchem-1252	228	73	(	(	PUNCT
eurjchem-1252	228	74	scheme	scheme	NOUN
eurjchem-1252	228	75	3	3	NUM
eurjchem-1252	228	76	)	)	PUNCT
eurjchem-1252	228	77	.	.	PUNCT
eurjchem-1252	229	1	color	color	NOUN
eurjchem-1252	229	2	:	:	PUNCT
eurjchem-1252	229	3	yellow	yellow	ADJ
eurjchem-1252	229	4	.	.	PUNCT
eurjchem-1252	230	1	yield	yield	NOUN
eurjchem-1252	230	2	:	:	PUNCT
eurjchem-1252	230	3	68.11	68.11	NUM
eurjchem-1252	230	4	%	%	NOUN
eurjchem-1252	230	5	.	.	PUNCT
eurjchem-1252	231	1	m.p	m.p	PROPN
eurjchem-1252	231	2	.	.	PROPN
eurjchem-1252	231	3	:	:	PUNCT
eurjchem-1252	232	1	>	>	X
eurjchem-1252	232	2	300	300	NUM
eurjchem-1252	232	3	°	°	SYM
eurjchem-1252	232	4	c	c	NOUN
eurjchem-1252	232	5	.	.	PUNCT
eurjchem-1252	233	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	233	2	(	(	PUNCT
eurjchem-1252	233	3	kbr	kbr	PROPN
eurjchem-1252	233	4	,	,	PUNCT
eurjchem-1252	233	5	ν	ν	PROPN
eurjchem-1252	233	6	,	,	PUNCT
eurjchem-1252	233	7	cm‐1	cm‐1	PROPN
eurjchem-1252	233	8	):	):	PUNCT
eurjchem-1252	233	9	3372	3372	NUM
eurjchem-1252	233	10	(	(	PUNCT
eurjchem-1252	233	11	oh	oh	INTJ
eurjchem-1252	233	12	)	)	PUNCT
eurjchem-1252	233	13	,	,	PUNCT
eurjchem-1252	233	14	3057	3057	NUM
eurjchem-1252	233	15	,	,	PUNCT
eurjchem-1252	233	16	3028	3028	NUM
eurjchem-1252	233	17	(	(	PUNCT
eurjchem-1252	233	18	ch	ch	NOUN
eurjchem-1252	233	19	,	,	PUNCT
eurjchem-1252	233	20	arom	arom	NOUN
eurjchem-1252	233	21	.	.	PUNCT
eurjchem-1252	233	22	)	)	PUNCT
eurjchem-1252	233	23	,	,	PUNCT
eurjchem-1252	233	24	1695	1695	NUM
eurjchem-1252	233	25	(	(	PUNCT
eurjchem-1252	233	26	c	c	NOUN
eurjchem-1252	233	27	=	=	NOUN
eurjchem-1252	233	28	o	o	NOUN
eurjchem-1252	233	29	)	)	PUNCT
eurjchem-1252	233	30	,	,	PUNCT
eurjchem-1252	233	31	1645	1645	NUM
eurjchem-1252	233	32	(	(	PUNCT
eurjchem-1252	233	33	c	c	NOUN
eurjchem-1252	233	34	=	=	SYM
eurjchem-1252	233	35	n	n	NUM
eurjchem-1252	233	36	)	)	PUNCT
eurjchem-1252	233	37	.	.	PUNCT
eurjchem-1252	234	1	ms	ms	NOUN
eurjchem-1252	234	2	(	(	PUNCT
eurjchem-1252	234	3	ei	ei	PROPN
eurjchem-1252	234	4	,	,	PUNCT
eurjchem-1252	234	5	m	m	PROPN
eurjchem-1252	234	6	/	/	SYM
eurjchem-1252	234	7	z	z	PROPN
eurjchem-1252	234	8	(	(	PUNCT
eurjchem-1252	234	9	%	%	NOUN
eurjchem-1252	234	10	)	)	PUNCT
eurjchem-1252	234	11	):	):	PUNCT
eurjchem-1252	234	12	521	521	NUM
eurjchem-1252	234	13	(	(	PUNCT
eurjchem-1252	234	14	m+	m+	NUM
eurjchem-1252	234	15	,	,	PUNCT
eurjchem-1252	234	16	6.45	6.45	NUM
eurjchem-1252	234	17	)	)	PUNCT
eurjchem-1252	234	18	,	,	PUNCT
eurjchem-1252	234	19	504	504	NUM
eurjchem-1252	234	20	(	(	PUNCT
eurjchem-1252	234	21	0.95	0.95	NUM
eurjchem-1252	234	22	)	)	PUNCT
eurjchem-1252	234	23	,	,	PUNCT
eurjchem-1252	234	24	444	444	NUM
eurjchem-1252	234	25	(	(	PUNCT
eurjchem-1252	234	26	2.50	2.50	NUM
eurjchem-1252	234	27	)	)	PUNCT
eurjchem-1252	234	28	,	,	PUNCT
eurjchem-1252	234	29	427	427	NUM
eurjchem-1252	234	30	(	(	PUNCT
eurjchem-1252	234	31	3.68	3.68	NUM
eurjchem-1252	234	32	)	)	PUNCT
eurjchem-1252	234	33	,	,	PUNCT
eurjchem-1252	234	34	416	416	NUM
eurjchem-1252	234	35	(	(	PUNCT
eurjchem-1252	234	36	7.77	7.77	NUM
eurjchem-1252	234	37	)	)	PUNCT
eurjchem-1252	234	38	,	,	PUNCT
eurjchem-1252	234	39	349	349	NUM
eurjchem-1252	234	40	(	(	PUNCT
eurjchem-1252	234	41	13.68	13.68	NUM
eurjchem-1252	234	42	)	)	PUNCT
eurjchem-1252	234	43	,	,	PUNCT
eurjchem-1252	234	44	334	334	NUM
eurjchem-1252	234	45	(	(	PUNCT
eurjchem-1252	234	46	33.44	33.44	NUM
eurjchem-1252	234	47	)	)	PUNCT
eurjchem-1252	234	48	,	,	PUNCT
eurjchem-1252	234	49	186	186	NUM
eurjchem-1252	234	50	(	(	PUNCT
eurjchem-1252	234	51	12.63	12.63	NUM
eurjchem-1252	234	52	)	)	PUNCT
eurjchem-1252	234	53	,	,	PUNCT
eurjchem-1252	234	54	178	178	NUM
eurjchem-1252	234	55	(	(	PUNCT
eurjchem-1252	234	56	20.22	20.22	NUM
eurjchem-1252	234	57	)	)	PUNCT
eurjchem-1252	234	58	,	,	PUNCT
eurjchem-1252	234	59	103	103	NUM
eurjchem-1252	234	60	(	(	PUNCT
eurjchem-1252	234	61	100	100	NUM
eurjchem-1252	234	62	)	)	PUNCT
eurjchem-1252	234	63	,	,	PUNCT
eurjchem-1252	234	64	76	76	NUM
eurjchem-1252	234	65	(	(	PUNCT
eurjchem-1252	234	66	37.66	37.66	NUM
eurjchem-1252	234	67	)	)	PUNCT
eurjchem-1252	234	68	.	.	PUNCT
eurjchem-1252	235	1	anal	anal	PROPN
eurjchem-1252	235	2	.	.	PUNCT
eurjchem-1252	235	3	calcd	calcd	NOUN
eurjchem-1252	235	4	.	.	PUNCT
eurjchem-1252	236	1	for	for	ADP
eurjchem-1252	236	2	c34h23n3o3	c34h23n3o3	PROPN
eurjchem-1252	236	3	:	:	PUNCT
eurjchem-1252	236	4	c	c	X
eurjchem-1252	236	5	,	,	PUNCT
eurjchem-1252	236	6	78.30	78.30	NUM
eurjchem-1252	236	7	;	;	PUNCT
eurjchem-1252	236	8	h	h	NOUN
eurjchem-1252	236	9	,	,	PUNCT
eurjchem-1252	236	10	4.44	4.44	NUM
eurjchem-1252	236	11	;	;	PUNCT
eurjchem-1252	236	12	n	n	CCONJ
eurjchem-1252	236	13	,	,	PUNCT
eurjchem-1252	236	14	8.06	8.06	NUM
eurjchem-1252	236	15	.	.	PUNCT
eurjchem-1252	236	16	found	find	VERB
eurjchem-1252	236	17	:	:	PUNCT
eurjchem-1252	237	1	c	c	X
eurjchem-1252	237	2	,	,	PUNCT
eurjchem-1252	237	3	78.51	78.51	NUM
eurjchem-1252	237	4	;	;	PUNCT
eurjchem-1252	237	5	h	h	NOUN
eurjchem-1252	237	6	,	,	PUNCT
eurjchem-1252	237	7	4.59	4.59	NUM
eurjchem-1252	237	8	;	;	PUNCT
eurjchem-1252	237	9	n	n	CCONJ
eurjchem-1252	237	10	,	,	PUNCT
eurjchem-1252	237	11	8.26	8.26	NUM
eurjchem-1252	237	12	%	%	NOUN
eurjchem-1252	237	13	.	.	PUNCT
eurjchem-1252	238	1	2.2.17	2.2.17	X
eurjchem-1252	238	2	.	.	PUNCT
eurjchem-1252	238	3	synthesis	synthesis	NOUN
eurjchem-1252	238	4	of	of	ADP
eurjchem-1252	238	5	3‐acetyl‐2‐chloro‐7,8,9‐triphenyl‐4h‐	3‐acetyl‐2‐chloro‐7,8,9‐triphenyl‐4h‐	NUM
eurjchem-1252	238	6	pyrimido[1,2‐b]pyridazin‐4‐one	pyrimido[1,2‐b]pyridazin‐4‐one	NOUN
eurjchem-1252	238	7	(	(	PUNCT
eurjchem-1252	238	8	14	14	NUM
eurjchem-1252	238	9	)	)	PUNCT
eurjchem-1252	238	10	a	a	DET
eurjchem-1252	238	11	mixture	mixture	NOUN
eurjchem-1252	238	12	of	of	ADP
eurjchem-1252	238	13	compound	compound	NOUN
eurjchem-1252	238	14	12	12	NUM
eurjchem-1252	238	15	(	(	PUNCT
eurjchem-1252	238	16	0.5	0.5	NUM
eurjchem-1252	238	17	g	g	NOUN
eurjchem-1252	238	18	,	,	PUNCT
eurjchem-1252	238	19	1.15	1.15	NUM
eurjchem-1252	238	20	mmol	mmol	NOUN
eurjchem-1252	238	21	)	)	PUNCT
eurjchem-1252	238	22	and	and	CCONJ
eurjchem-1252	238	23	phosphoryl	phosphoryl	PROPN
eurjchem-1252	238	24	chloride	chloride	PROPN
eurjchem-1252	238	25	(	(	PUNCT
eurjchem-1252	238	26	10	10	NUM
eurjchem-1252	238	27	ml	ml	NOUN
eurjchem-1252	238	28	)	)	PUNCT
eurjchem-1252	238	29	was	be	AUX
eurjchem-1252	238	30	refluxed	refluxe	VERB
eurjchem-1252	238	31	for	for	ADP
eurjchem-1252	238	32	3	3	NUM
eurjchem-1252	238	33	h.	h.	NOUN
eurjchem-1252	238	34	the	the	DET
eurjchem-1252	238	35	reaction	reaction	NOUN
eurjchem-1252	238	36	mixture	mixture	NOUN
eurjchem-1252	238	37	was	be	AUX
eurjchem-1252	238	38	cooled	cool	VERB
eurjchem-1252	238	39	,	,	PUNCT
eurjchem-1252	238	40	and	and	CCONJ
eurjchem-1252	238	41	poured	pour	VERB
eurjchem-1252	238	42	into	into	ADP
eurjchem-1252	238	43	ice	ice	NOUN
eurjchem-1252	238	44	water	water	NOUN
eurjchem-1252	238	45	(	(	PUNCT
eurjchem-1252	238	46	200	200	NUM
eurjchem-1252	238	47	ml	ml	NOUN
eurjchem-1252	238	48	)	)	PUNCT
eurjchem-1252	238	49	.	.	PUNCT
eurjchem-1252	239	1	the	the	DET
eurjchem-1252	239	2	solid	solid	ADJ
eurjchem-1252	239	3	product	product	NOUN
eurjchem-1252	239	4	was	be	AUX
eurjchem-1252	239	5	filtered	filter	VERB
eurjchem-1252	239	6	off	off	ADP
eurjchem-1252	239	7	,	,	PUNCT
eurjchem-1252	239	8	washed	wash	VERB
eurjchem-1252	239	9	with	with	ADP
eurjchem-1252	239	10	water	water	NOUN
eurjchem-1252	239	11	,	,	PUNCT
eurjchem-1252	239	12	dried	dry	VERB
eurjchem-1252	239	13	,	,	PUNCT
eurjchem-1252	239	14	and	and	CCONJ
eurjchem-1252	239	15	recrystallized	recrystallize	VERB
eurjchem-1252	239	16	from	from	ADP
eurjchem-1252	239	17	ethanol	ethanol	NOUN
eurjchem-1252	239	18	to	to	PART
eurjchem-1252	239	19	give	give	VERB
eurjchem-1252	239	20	compound	compound	NOUN
eurjchem-1252	239	21	14	14	NUM
eurjchem-1252	239	22	(	(	PUNCT
eurjchem-1252	239	23	scheme	scheme	NOUN
eurjchem-1252	239	24	3	3	NUM
eurjchem-1252	239	25	)	)	PUNCT
eurjchem-1252	239	26	.	.	PUNCT
eurjchem-1252	240	1	color	color	NOUN
eurjchem-1252	240	2	:	:	PUNCT
eurjchem-1252	240	3	reddish	reddish	PROPN
eurjchem-1252	240	4	brown	brown	NOUN
eurjchem-1252	240	5	.	.	PUNCT
eurjchem-1252	241	1	yield	yield	NOUN
eurjchem-1252	241	2	:	:	PUNCT
eurjchem-1252	241	3	65.22	65.22	NUM
eurjchem-1252	241	4	%	%	NOUN
eurjchem-1252	241	5	.	.	PUNCT
eurjchem-1252	242	1	m.p	m.p	PROPN
eurjchem-1252	242	2	.	.	PROPN
eurjchem-1252	242	3	:	:	PUNCT
eurjchem-1252	243	1	175‐177	175‐177	NUM
eurjchem-1252	243	2	°	°	ADP
eurjchem-1252	243	3	c	c	X
eurjchem-1252	243	4	.	.	PUNCT
eurjchem-1252	244	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	244	2	(	(	PUNCT
eurjchem-1252	244	3	kbr	kbr	PROPN
eurjchem-1252	244	4	,	,	PUNCT
eurjchem-1252	244	5	ν	ν	PROPN
eurjchem-1252	244	6	,	,	PUNCT
eurjchem-1252	244	7	cm‐1	cm‐1	PROPN
eurjchem-1252	244	8	):	):	PUNCT
eurjchem-1252	244	9	3058	3058	NUM
eurjchem-1252	244	10	(	(	PUNCT
eurjchem-1252	244	11	ch	ch	NOUN
eurjchem-1252	244	12	,	,	PUNCT
eurjchem-1252	244	13	arom	arom	NOUN
eurjchem-1252	244	14	.	.	PUNCT
eurjchem-1252	244	15	)	)	PUNCT
eurjchem-1252	244	16	,	,	PUNCT
eurjchem-1252	244	17	2923	2923	NUM
eurjchem-1252	244	18	,	,	PUNCT
eurjchem-1252	244	19	2853	2853	NUM
eurjchem-1252	244	20	(	(	PUNCT
eurjchem-1252	244	21	ch	ch	NOUN
eurjchem-1252	244	22	,	,	PUNCT
eurjchem-1252	244	23	aliph	aliph	NOUN
eurjchem-1252	244	24	.	.	PUNCT
eurjchem-1252	244	25	)	)	PUNCT
eurjchem-1252	245	1	,	,	PUNCT
eurjchem-1252	245	2	1717	1717	NUM
eurjchem-1252	245	3	(	(	PUNCT
eurjchem-1252	245	4	c	c	NOUN
eurjchem-1252	245	5	=	=	NOUN
eurjchem-1252	245	6	o	o	NOUN
eurjchem-1252	245	7	)	)	PUNCT
eurjchem-1252	245	8	,	,	PUNCT
eurjchem-1252	245	9	1619	1619	NUM
eurjchem-1252	245	10	(	(	PUNCT
eurjchem-1252	245	11	c	c	NOUN
eurjchem-1252	245	12	=	=	SYM
eurjchem-1252	245	13	n	n	NUM
eurjchem-1252	245	14	)	)	PUNCT
eurjchem-1252	245	15	.	.	PUNCT
eurjchem-1252	246	1	1h	1h	NUM
eurjchem-1252	246	2	nmr	nmr	NOUN
eurjchem-1252	246	3	(	(	PUNCT
eurjchem-1252	246	4	300	300	NUM
eurjchem-1252	246	5	mhz	mhz	NOUN
eurjchem-1252	246	6	,	,	PUNCT
eurjchem-1252	246	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1252	246	8	,	,	PUNCT
eurjchem-1252	246	9	δ	δ	PROPN
eurjchem-1252	246	10	,	,	PUNCT
eurjchem-1252	246	11	ppm	ppm	NOUN
eurjchem-1252	246	12	):	):	PUNCT
eurjchem-1252	246	13	2.09	2.09	NUM
eurjchem-1252	246	14	(	(	PUNCT
eurjchem-1252	246	15	s	s	PROPN
eurjchem-1252	246	16	,	,	PUNCT
eurjchem-1252	246	17	3h	3h	NUM
eurjchem-1252	246	18	,	,	PUNCT
eurjchem-1252	246	19	ch3	ch3	PROPN
eurjchem-1252	246	20	)	)	PUNCT
eurjchem-1252	246	21	,	,	PUNCT
eurjchem-1252	246	22	6.99‐7.63	6.99‐7.63	NUM
eurjchem-1252	246	23	(	(	PUNCT
eurjchem-1252	246	24	m	m	PROPN
eurjchem-1252	246	25	,	,	PUNCT
eurjchem-1252	246	26	15h	15h	NUM
eurjchem-1252	246	27	,	,	PUNCT
eurjchem-1252	246	28	3ph	3ph	NOUN
eurjchem-1252	246	29	)	)	PUNCT
eurjchem-1252	246	30	.	.	PUNCT
eurjchem-1252	247	1	ms	ms	NOUN
eurjchem-1252	247	2	(	(	PUNCT
eurjchem-1252	247	3	ei	ei	PROPN
eurjchem-1252	247	4	,	,	PUNCT
eurjchem-1252	247	5	m	m	PROPN
eurjchem-1252	247	6	/	/	SYM
eurjchem-1252	247	7	z	z	PROPN
eurjchem-1252	247	8	(	(	PUNCT
eurjchem-1252	247	9	%	%	NOUN
eurjchem-1252	247	10	)	)	PUNCT
eurjchem-1252	247	11	):	):	PUNCT
eurjchem-1252	247	12	454	454	NUM
eurjchem-1252	247	13	(	(	PUNCT
eurjchem-1252	247	14	m+	m+	NOUN
eurjchem-1252	247	15	+	+	CCONJ
eurjchem-1252	247	16	2	2	NUM
eurjchem-1252	247	17	,	,	PUNCT
eurjchem-1252	247	18	0.34	0.34	NUM
eurjchem-1252	247	19	)	)	PUNCT
eurjchem-1252	247	20	,	,	PUNCT
eurjchem-1252	247	21	452	452	NUM
eurjchem-1252	247	22	(	(	PUNCT
eurjchem-1252	247	23	m+	m+	NUM
eurjchem-1252	247	24	,	,	PUNCT
eurjchem-1252	247	25	0.38	0.38	NUM
eurjchem-1252	247	26	)	)	PUNCT
eurjchem-1252	247	27	,	,	PUNCT
eurjchem-1252	247	28	437	437	NUM
eurjchem-1252	247	29	(	(	PUNCT
eurjchem-1252	247	30	4.81	4.81	NUM
eurjchem-1252	247	31	)	)	PUNCT
eurjchem-1252	247	32	,	,	PUNCT
eurjchem-1252	247	33	409	409	NUM
eurjchem-1252	247	34	(	(	PUNCT
eurjchem-1252	247	35	33.37	33.37	NUM
eurjchem-1252	247	36	)	)	PUNCT
eurjchem-1252	247	37	,	,	PUNCT
eurjchem-1252	247	38	408	408	NUM
eurjchem-1252	247	39	(	(	PUNCT
eurjchem-1252	247	40	100	100	NUM
eurjchem-1252	247	41	)	)	PUNCT
eurjchem-1252	247	42	,	,	PUNCT
eurjchem-1252	247	43	375	375	NUM
eurjchem-1252	247	44	(	(	PUNCT
eurjchem-1252	247	45	0.63	0.63	NUM
eurjchem-1252	247	46	)	)	PUNCT
eurjchem-1252	247	47	,	,	PUNCT
eurjchem-1252	247	48	349	349	NUM
eurjchem-1252	247	49	(	(	PUNCT
eurjchem-1252	247	50	23.65	23.65	NUM
eurjchem-1252	247	51	)	)	PUNCT
eurjchem-1252	247	52	,	,	PUNCT
eurjchem-1252	247	53	281	281	NUM
eurjchem-1252	247	54	(	(	PUNCT
eurjchem-1252	247	55	8.56	8.56	NUM
eurjchem-1252	247	56	)	)	PUNCT
eurjchem-1252	247	57	,	,	PUNCT
eurjchem-1252	247	58	274	274	NUM
eurjchem-1252	247	59	(	(	PUNCT
eurjchem-1252	247	60	2.79	2.79	NUM
eurjchem-1252	247	61	)	)	PUNCT
eurjchem-1252	247	62	,	,	PUNCT
eurjchem-1252	247	63	178	178	NUM
eurjchem-1252	247	64	(	(	PUNCT
eurjchem-1252	247	65	6.63	6.63	NUM
eurjchem-1252	247	66	)	)	PUNCT
eurjchem-1252	247	67	,	,	PUNCT
eurjchem-1252	247	68	171	171	NUM
eurjchem-1252	247	69	(	(	PUNCT
eurjchem-1252	247	70	2.55	2.55	NUM
eurjchem-1252	247	71	)	)	PUNCT
eurjchem-1252	247	72	,	,	PUNCT
eurjchem-1252	247	73	103	103	NUM
eurjchem-1252	247	74	(	(	PUNCT
eurjchem-1252	247	75	22.60	22.60	NUM
eurjchem-1252	247	76	)	)	PUNCT
eurjchem-1252	247	77	,	,	PUNCT
eurjchem-1252	247	78	77	77	NUM
eurjchem-1252	247	79	(	(	PUNCT
eurjchem-1252	247	80	23.94	23.94	NUM
eurjchem-1252	247	81	)	)	PUNCT
eurjchem-1252	247	82	.	.	PUNCT
eurjchem-1252	248	1	anal	anal	PROPN
eurjchem-1252	248	2	.	.	PUNCT
eurjchem-1252	248	3	calcd	calcd	NOUN
eurjchem-1252	248	4	.	.	PUNCT
eurjchem-1252	249	1	for	for	SCONJ
eurjchem-1252	249	2	c27h18cln3o2	c27h18cln3o2	PROPN
eurjchem-1252	249	3	:	:	PUNCT
eurjchem-1252	249	4	c	c	X
eurjchem-1252	249	5	,	,	PUNCT
eurjchem-1252	249	6	71.76	71.76	NUM
eurjchem-1252	249	7	;	;	PUNCT
eurjchem-1252	249	8	h	h	NOUN
eurjchem-1252	249	9	,	,	PUNCT
eurjchem-1252	249	10	4.01	4.01	NUM
eurjchem-1252	249	11	;	;	PUNCT
eurjchem-1252	249	12	n	n	CCONJ
eurjchem-1252	249	13	,	,	PUNCT
eurjchem-1252	249	14	9.30	9.30	NUM
eurjchem-1252	249	15	.	.	PUNCT
eurjchem-1252	249	16	found	find	VERB
eurjchem-1252	249	17	:	:	PUNCT
eurjchem-1252	250	1	c	c	X
eurjchem-1252	250	2	,	,	PUNCT
eurjchem-1252	250	3	71.98	71.98	NUM
eurjchem-1252	250	4	;	;	PUNCT
eurjchem-1252	250	5	h	h	NOUN
eurjchem-1252	250	6	,	,	PUNCT
eurjchem-1252	250	7	4.12	4.12	NUM
eurjchem-1252	250	8	;	;	PUNCT
eurjchem-1252	250	9	n	n	CCONJ
eurjchem-1252	250	10	,	,	PUNCT
eurjchem-1252	250	11	9.48	9.48	NUM
eurjchem-1252	250	12	%	%	NOUN
eurjchem-1252	250	13	.	.	PUNCT
eurjchem-1252	251	1	2.2.18	2.2.18	NUM
eurjchem-1252	251	2	.	.	PUNCT
eurjchem-1252	251	3	synthesis	synthesis	NOUN
eurjchem-1252	251	4	of	of	ADP
eurjchem-1252	251	5	2,3,4‐triphenylpyrano[2',3':4,5	2,3,4‐triphenylpyrano[2',3':4,5	NUM
eurjchem-1252	251	6	]	]	X
eurjchem-1252	251	7	pyrimido[1,2‐b]pyridazine‐7,9,10(8h)‐trione	pyrimido[1,2‐b]pyridazine‐7,9,10(8h)‐trione	NOUN
eurjchem-1252	251	8	(	(	PUNCT
eurjchem-1252	251	9	15	15	NUM
eurjchem-1252	251	10	)	)	PUNCT
eurjchem-1252	251	11	a	a	DET
eurjchem-1252	251	12	mixture	mixture	NOUN
eurjchem-1252	251	13	of	of	ADP
eurjchem-1252	251	14	compound	compound	NOUN
eurjchem-1252	251	15	1	1	NUM
eurjchem-1252	251	16	(	(	PUNCT
eurjchem-1252	251	17	0.5	0.5	NUM
eurjchem-1252	251	18	g	g	NOUN
eurjchem-1252	251	19	,	,	PUNCT
eurjchem-1252	251	20	1.28	1.28	NUM
eurjchem-1252	251	21	mmol	mmol	NOUN
eurjchem-1252	251	22	)	)	PUNCT
eurjchem-1252	251	23	and	and	CCONJ
eurjchem-1252	251	24	diethyl	diethyl	NOUN
eurjchem-1252	251	25	malonate	malonate	NOUN
eurjchem-1252	251	26	(	(	PUNCT
eurjchem-1252	251	27	1.28	1.28	NUM
eurjchem-1252	251	28	mmol	mmol	NOUN
eurjchem-1252	251	29	)	)	PUNCT
eurjchem-1252	251	30	was	be	AUX
eurjchem-1252	251	31	refluxed	refluxe	VERB
eurjchem-1252	251	32	for	for	ADP
eurjchem-1252	251	33	3	3	NUM
eurjchem-1252	251	34	h.	h.	NOUN
eurjchem-1252	251	35	208	208	NUM
eurjchem-1252	251	36	deeb	deeb	PROPN
eurjchem-1252	251	37	et	et	PROPN
eurjchem-1252	251	38	al	al	PROPN
eurjchem-1252	251	39	.	.	PUNCT
eurjchem-1252	251	40	/	/	SYM
eurjchem-1252	251	41	european	european	PROPN
eurjchem-1252	251	42	journal	journal	PROPN
eurjchem-1252	251	43	of	of	ADP
eurjchem-1252	251	44	chemistry	chemistry	NOUN
eurjchem-1252	251	45	6	6	NUM
eurjchem-1252	251	46	(	(	PUNCT
eurjchem-1252	251	47	2	2	NUM
eurjchem-1252	251	48	)	)	PUNCT
eurjchem-1252	251	49	(	(	PUNCT
eurjchem-1252	251	50	2015	2015	NUM
eurjchem-1252	251	51	)	)	PUNCT
eurjchem-1252	251	52	204‐210	204‐210	NOUN
eurjchem-1252	251	53	n	n	CCONJ
eurjchem-1252	251	54	n	n	CCONJ
eurjchem-1252	251	55	n	n	NOUN
eurjchem-1252	251	56	o	o	NOUN
eurjchem-1252	251	57	o	o	X
eurjchem-1252	251	58	ph	ph	NOUN
eurjchem-1252	251	59	ph	ph	NOUN
eurjchem-1252	251	60	ph	ph	NOUN
eurjchem-1252	252	1	oh	oh	INTJ
eurjchem-1252	252	2	ph	ph	PROPN
eurjchem-1252	252	3	13	13	NUM
eurjchem-1252	252	4	n	n	CCONJ
eurjchem-1252	252	5	n	n	CCONJ
eurjchem-1252	252	6	n	n	ADV
eurjchem-1252	252	7	o	o	X
eurjchem-1252	252	8	ph	ph	ADJ
eurjchem-1252	252	9	ph	ph	NOUN
eurjchem-1252	252	10	ph	ph	NOUN
eurjchem-1252	252	11	o	o	NOUN
eurjchem-1252	252	12	o	o	NOUN
eurjchem-1252	252	13	o	o	NOUN
eurjchem-1252	252	14	15	15	NUM
eurjchem-1252	252	15	n	n	CCONJ
eurjchem-1252	252	16	n	n	CCONJ
eurjchem-1252	252	17	n	n	NOUN
eurjchem-1252	252	18	o	o	NOUN
eurjchem-1252	252	19	o	o	X
eurjchem-1252	252	20	ph	ph	NOUN
eurjchem-1252	252	21	ph	ph	NOUN
eurjchem-1252	252	22	ph	ph	NOUN
eurjchem-1252	253	1	oh	oh	INTJ
eurjchem-1252	253	2	h	h	NOUN
eurjchem-1252	253	3	16	16	NUM
eurjchem-1252	253	4	n	n	CCONJ
eurjchem-1252	253	5	n	n	CCONJ
eurjchem-1252	253	6	n	n	NOUN
eurjchem-1252	253	7	o	o	PROPN
eurjchem-1252	253	8	cl	cl	NOUN
eurjchem-1252	253	9	ph	ph	VERB
eurjchem-1252	253	10	ph	ph	ADJ
eurjchem-1252	253	11	ph	ph	PROPN
eurjchem-1252	253	12	cho	cho	NOUN
eurjchem-1252	253	13	17	17	NUM
eurjchem-1252	253	14	14	14	NUM
eurjchem-1252	253	15	n	n	CCONJ
eurjchem-1252	253	16	n	n	PRON
eurjchem-1252	253	17	ph	ph	ADJ
eurjchem-1252	253	18	ph	ph	NOUN
eurjchem-1252	253	19	ph	ph	NOUN
eurjchem-1252	253	20	n	n	ADP
eurjchem-1252	253	21	cl	cl	NOUN
eurjchem-1252	253	22	o	o	X
eurjchem-1252	253	23	coch3	coch3	PROPN
eurjchem-1252	253	24	n	n	CCONJ
eurjchem-1252	253	25	n	n	CCONJ
eurjchem-1252	253	26	n	n	ADV
eurjchem-1252	253	27	o	o	NOUN
eurjchem-1252	253	28	o	o	X
eurjchem-1252	253	29	ph	ph	NOUN
eurjchem-1252	253	30	ph	ph	NOUN
eurjchem-1252	253	31	ph	ph	NOUN
eurjchem-1252	253	32	oh	oh	INTJ
eurjchem-1252	253	33	ch3	ch3	PROPN
eurjchem-1252	253	34	12	12	NUM
eurjchem-1252	253	35	phcho	phcho	PROPN
eurjchem-1252	253	36	/	/	SYM
eurjchem-1252	253	37	naoh	naoh	PROPN
eurjchem-1252	253	38	/	/	SYM
eurjchem-1252	253	39	etoh	etoh	PROPN
eurjchem-1252	253	40	stirring	stirring	NOUN
eurjchem-1252	253	41	at	at	ADP
eurjchem-1252	253	42	r.t	r.t	PROPN
eurjchem-1252	253	43	.	.	PROPN
eurjchem-1252	254	1	for	for	ADP
eurjchem-1252	254	2	1	1	NUM
eurjchem-1252	254	3	h	h	PROPN
eurjchem-1252	254	4	dem	dem	NOUN
eurjchem-1252	254	5	,	,	PUNCT
eurjchem-1252	254	6	fusion	fusion	NOUN
eurjchem-1252	254	7	3	3	NUM
eurjchem-1252	254	8	h	h	NOUN
eurjchem-1252	254	9	reflux	reflux	NOUN
eurjchem-1252	254	10	3	3	NUM
eurjchem-1252	254	11	h.	h.	PROPN
eurjchem-1252	254	12	koh	koh	PROPN
eurjchem-1252	254	13	/	/	PUNCT
eurjchem-1252	254	14	chcl3	chcl3	PROPN
eurjchem-1252	254	15	reflux	reflux	VERB
eurjchem-1252	254	16	12	12	NUM
eurjchem-1252	254	17	h	h	NOUN
eurjchem-1252	254	18	stirring	stir	VERB
eurjchem-1252	254	19	at	at	ADP
eurjchem-1252	254	20	60	60	NUM
eurjchem-1252	254	21	oc	oc	NOUN
eurjchem-1252	254	22	,	,	PUNCT
eurjchem-1252	254	23	for	for	ADP
eurjchem-1252	254	24	2h	2h	NUM
eurjchem-1252	254	25	acoh/	acoh/	NUM
eurjchem-1252	254	26	ppa	ppa	PROPN
eurjchem-1252	254	27	,	,	PUNCT
eurjchem-1252	254	28	reflux	reflux	NOUN
eurjchem-1252	254	29	2	2	NUM
eurjchem-1252	254	30	h	h	NOUN
eurjchem-1252	254	31	reflux	reflux	NOUN
eurjchem-1252	254	32	1	1	NUM
eurjchem-1252	254	33	hpocl3	hpocl3	PROPN
eurjchem-1252	254	34	pocl3	pocl3	PROPN
eurjchem-1252	254	35	/	/	SYM
eurjchem-1252	254	36	dmf	dmf	PROPN
eurjchem-1252	254	37	pocl3	pocl3	X
eurjchem-1252	254	38	n	n	CCONJ
eurjchem-1252	254	39	n	n	CCONJ
eurjchem-1252	254	40	n	n	ADV
eurjchem-1252	254	41	o	o	NOUN
eurjchem-1252	254	42	o	o	X
eurjchem-1252	254	43	ph	ph	NOUN
eurjchem-1252	254	44	ph	ph	ADJ
eurjchem-1252	254	45	ph	ph	NOUN
eurjchem-1252	254	46	1	1	NUM
eurjchem-1252	254	47	scheme	scheme	NOUN
eurjchem-1252	254	48	3	3	NUM
eurjchem-1252	254	49	the	the	DET
eurjchem-1252	254	50	reaction	reaction	NOUN
eurjchem-1252	254	51	mixture	mixture	NOUN
eurjchem-1252	254	52	was	be	AUX
eurjchem-1252	254	53	cooled	cool	VERB
eurjchem-1252	254	54	,	,	PUNCT
eurjchem-1252	254	55	treated	treat	VERB
eurjchem-1252	254	56	with	with	ADP
eurjchem-1252	254	57	diethyl	diethyl	NOUN
eurjchem-1252	254	58	ether	ether	NOUN
eurjchem-1252	254	59	(	(	PUNCT
eurjchem-1252	254	60	50	50	NUM
eurjchem-1252	254	61	ml	ml	NOUN
eurjchem-1252	254	62	)	)	PUNCT
eurjchem-1252	254	63	,	,	PUNCT
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eurjchem-1252	254	65	the	the	DET
eurjchem-1252	254	66	solid	solid	ADJ
eurjchem-1252	254	67	product	product	NOUN
eurjchem-1252	254	68	was	be	AUX
eurjchem-1252	254	69	filtered	filter	VERB
eurjchem-1252	254	70	off	off	ADP
eurjchem-1252	254	71	,	,	PUNCT
eurjchem-1252	254	72	washed	wash	VERB
eurjchem-1252	254	73	with	with	ADP
eurjchem-1252	254	74	diethyl	diethyl	NOUN
eurjchem-1252	254	75	ether	ether	NOUN
eurjchem-1252	254	76	,	,	PUNCT
eurjchem-1252	254	77	dried	dry	VERB
eurjchem-1252	254	78	,	,	PUNCT
eurjchem-1252	254	79	and	and	CCONJ
eurjchem-1252	254	80	recrystallized	recrystallize	VERB
eurjchem-1252	254	81	from	from	ADP
eurjchem-1252	254	82	methanol	methanol	NOUN
eurjchem-1252	254	83	to	to	PART
eurjchem-1252	254	84	afford	afford	VERB
eurjchem-1252	254	85	compound	compound	VERB
eurjchem-1252	254	86	15	15	NUM
eurjchem-1252	254	87	(	(	PUNCT
eurjchem-1252	254	88	scheme	scheme	NOUN
eurjchem-1252	254	89	3	3	NUM
eurjchem-1252	254	90	)	)	PUNCT
eurjchem-1252	254	91	.	.	PUNCT
eurjchem-1252	255	1	color	color	NOUN
eurjchem-1252	255	2	:	:	PUNCT
eurjchem-1252	255	3	brown	brown	ADJ
eurjchem-1252	255	4	.	.	PUNCT
eurjchem-1252	256	1	yield	yield	NOUN
eurjchem-1252	256	2	:	:	PUNCT
eurjchem-1252	256	3	64.75	64.75	NUM
eurjchem-1252	256	4	%	%	NOUN
eurjchem-1252	256	5	.	.	PUNCT
eurjchem-1252	257	1	m.p	m.p	PROPN
eurjchem-1252	257	2	.	.	PROPN
eurjchem-1252	257	3	:	:	PUNCT
eurjchem-1252	258	1	174‐176	174‐176	PROPN
eurjchem-1252	258	2	°	°	ADP
eurjchem-1252	258	3	c	c	X
eurjchem-1252	258	4	.	.	PUNCT
eurjchem-1252	259	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	259	2	(	(	PUNCT
eurjchem-1252	259	3	kbr	kbr	PROPN
eurjchem-1252	259	4	,	,	PUNCT
eurjchem-1252	259	5	ν	ν	PROPN
eurjchem-1252	259	6	,	,	PUNCT
eurjchem-1252	259	7	cm‐1	cm‐1	PROPN
eurjchem-1252	259	8	):	):	PUNCT
eurjchem-1252	259	9	3057	3057	NUM
eurjchem-1252	259	10	(	(	PUNCT
eurjchem-1252	259	11	ch	ch	NOUN
eurjchem-1252	259	12	,	,	PUNCT
eurjchem-1252	259	13	arom	arom	NOUN
eurjchem-1252	259	14	.	.	PUNCT
eurjchem-1252	259	15	)	)	PUNCT
eurjchem-1252	259	16	,	,	PUNCT
eurjchem-1252	259	17	1707	1707	NUM
eurjchem-1252	259	18	(	(	PUNCT
eurjchem-1252	259	19	c	c	NOUN
eurjchem-1252	259	20	=	=	NOUN
eurjchem-1252	259	21	o	o	NOUN
eurjchem-1252	259	22	)	)	PUNCT
eurjchem-1252	259	23	,	,	PUNCT
eurjchem-1252	259	24	1646	1646	NUM
eurjchem-1252	259	25	(	(	PUNCT
eurjchem-1252	259	26	c	c	NOUN
eurjchem-1252	259	27	=	=	SYM
eurjchem-1252	259	28	n	n	NUM
eurjchem-1252	259	29	)	)	PUNCT
eurjchem-1252	259	30	.	.	PUNCT
eurjchem-1252	260	1	1h	1h	NUM
eurjchem-1252	260	2	nmr	nmr	NOUN
eurjchem-1252	260	3	(	(	PUNCT
eurjchem-1252	260	4	300	300	NUM
eurjchem-1252	260	5	mhz	mhz	NOUN
eurjchem-1252	260	6	,	,	PUNCT
eurjchem-1252	260	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1252	260	8	,	,	PUNCT
eurjchem-1252	260	9	δ	δ	PROPN
eurjchem-1252	260	10	,	,	PUNCT
eurjchem-1252	260	11	ppm	ppm	NOUN
eurjchem-1252	260	12	):	):	PUNCT
eurjchem-1252	260	13	4.11	4.11	NUM
eurjchem-1252	260	14	(	(	PUNCT
eurjchem-1252	260	15	s	s	PROPN
eurjchem-1252	260	16	,	,	PUNCT
eurjchem-1252	260	17	2h	2h	NUM
eurjchem-1252	260	18	,	,	PUNCT
eurjchem-1252	260	19	ch2	ch2	PROPN
eurjchem-1252	260	20	)	)	PUNCT
eurjchem-1252	260	21	,	,	PUNCT
eurjchem-1252	260	22	6.78‐7.65	6.78‐7.65	NUM
eurjchem-1252	260	23	(	(	PUNCT
eurjchem-1252	260	24	m	m	PROPN
eurjchem-1252	260	25	,	,	PUNCT
eurjchem-1252	260	26	15h	15h	NUM
eurjchem-1252	260	27	,	,	PUNCT
eurjchem-1252	260	28	3ph	3ph	NOUN
eurjchem-1252	260	29	)	)	PUNCT
eurjchem-1252	260	30	.	.	PUNCT
eurjchem-1252	261	1	ms	ms	NOUN
eurjchem-1252	261	2	(	(	PUNCT
eurjchem-1252	261	3	ei	ei	PROPN
eurjchem-1252	261	4	,	,	PUNCT
eurjchem-1252	261	5	m	m	PROPN
eurjchem-1252	261	6	/	/	SYM
eurjchem-1252	261	7	z	z	PROPN
eurjchem-1252	261	8	(	(	PUNCT
eurjchem-1252	261	9	%	%	NOUN
eurjchem-1252	261	10	)	)	PUNCT
eurjchem-1252	261	11	):	):	PUNCT
eurjchem-1252	261	12	459	459	NUM
eurjchem-1252	261	13	(	(	PUNCT
eurjchem-1252	261	14	m+	m+	NUM
eurjchem-1252	261	15	,	,	PUNCT
eurjchem-1252	261	16	1.47	1.47	NUM
eurjchem-1252	261	17	)	)	PUNCT
eurjchem-1252	261	18	,	,	PUNCT
eurjchem-1252	261	19	441	441	NUM
eurjchem-1252	261	20	(	(	PUNCT
eurjchem-1252	261	21	0.59	0.59	NUM
eurjchem-1252	261	22	)	)	PUNCT
eurjchem-1252	261	23	,	,	PUNCT
eurjchem-1252	261	24	431	431	NUM
eurjchem-1252	261	25	(	(	PUNCT
eurjchem-1252	261	26	1.24	1.24	NUM
eurjchem-1252	261	27	)	)	PUNCT
eurjchem-1252	261	28	,	,	PUNCT
eurjchem-1252	261	29	418	418	NUM
eurjchem-1252	261	30	(	(	PUNCT
eurjchem-1252	261	31	0.17	0.17	NUM
eurjchem-1252	261	32	)	)	PUNCT
eurjchem-1252	261	33	,	,	PUNCT
eurjchem-1252	261	34	414	414	NUM
eurjchem-1252	261	35	(	(	PUNCT
eurjchem-1252	261	36	0.98	0.98	NUM
eurjchem-1252	261	37	)	)	PUNCT
eurjchem-1252	261	38	,	,	PUNCT
eurjchem-1252	261	39	408	408	NUM
eurjchem-1252	261	40	(	(	PUNCT
eurjchem-1252	261	41	100	100	NUM
eurjchem-1252	261	42	)	)	PUNCT
eurjchem-1252	261	43	,	,	PUNCT
eurjchem-1252	261	44	398	398	NUM
eurjchem-1252	261	45	(	(	PUNCT
eurjchem-1252	261	46	3.56	3.56	NUM
eurjchem-1252	261	47	)	)	PUNCT
eurjchem-1252	261	48	,	,	PUNCT
eurjchem-1252	261	49	382	382	NUM
eurjchem-1252	261	50	(	(	PUNCT
eurjchem-1252	261	51	3.13	3.13	NUM
eurjchem-1252	261	52	)	)	PUNCT
eurjchem-1252	261	53	,	,	PUNCT
eurjchem-1252	261	54	373	373	NUM
eurjchem-1252	261	55	(	(	PUNCT
eurjchem-1252	261	56	2.64	2.64	NUM
eurjchem-1252	261	57	)	)	PUNCT
eurjchem-1252	261	58	,	,	PUNCT
eurjchem-1252	261	59	356	356	NUM
eurjchem-1252	261	60	(	(	PUNCT
eurjchem-1252	261	61	0.84	0.84	NUM
eurjchem-1252	261	62	)	)	PUNCT
eurjchem-1252	261	63	,	,	PUNCT
eurjchem-1252	261	64	349	349	NUM
eurjchem-1252	261	65	(	(	PUNCT
eurjchem-1252	261	66	1.59	1.59	NUM
eurjchem-1252	261	67	)	)	PUNCT
eurjchem-1252	261	68	,	,	PUNCT
eurjchem-1252	261	69	307	307	NUM
eurjchem-1252	261	70	(	(	PUNCT
eurjchem-1252	261	71	3.97	3.97	NUM
eurjchem-1252	261	72	)	)	PUNCT
eurjchem-1252	261	73	,	,	PUNCT
eurjchem-1252	261	74	281	281	NUM
eurjchem-1252	261	75	(	(	PUNCT
eurjchem-1252	261	76	0.18	0.18	NUM
eurjchem-1252	261	77	)	)	PUNCT
eurjchem-1252	261	78	,	,	PUNCT
eurjchem-1252	261	79	253	253	NUM
eurjchem-1252	261	80	(	(	PUNCT
eurjchem-1252	261	81	0.66	0.66	NUM
eurjchem-1252	261	82	)	)	PUNCT
eurjchem-1252	261	83	,	,	PUNCT
eurjchem-1252	261	84	231	231	NUM
eurjchem-1252	261	85	(	(	PUNCT
eurjchem-1252	261	86	0.47	0.47	NUM
eurjchem-1252	261	87	)	)	PUNCT
eurjchem-1252	261	88	,	,	PUNCT
eurjchem-1252	261	89	178	178	NUM
eurjchem-1252	261	90	(	(	PUNCT
eurjchem-1252	261	91	10.91	10.91	NUM
eurjchem-1252	261	92	)	)	PUNCT
eurjchem-1252	261	93	,	,	PUNCT
eurjchem-1252	261	94	152	152	NUM
eurjchem-1252	261	95	(	(	PUNCT
eurjchem-1252	261	96	3.47	3.47	NUM
eurjchem-1252	261	97	)	)	PUNCT
eurjchem-1252	261	98	,	,	PUNCT
eurjchem-1252	261	99	110	110	NUM
eurjchem-1252	261	100	(	(	PUNCT
eurjchem-1252	261	101	0.69	0.69	NUM
eurjchem-1252	261	102	)	)	PUNCT
eurjchem-1252	261	103	,	,	PUNCT
eurjchem-1252	261	104	103	103	NUM
eurjchem-1252	261	105	(	(	PUNCT
eurjchem-1252	261	106	2.57	2.57	NUM
eurjchem-1252	261	107	)	)	PUNCT
eurjchem-1252	261	108	,	,	PUNCT
eurjchem-1252	261	109	86	86	NUM
eurjchem-1252	261	110	(	(	PUNCT
eurjchem-1252	261	111	1.46	1.46	NUM
eurjchem-1252	261	112	)	)	PUNCT
eurjchem-1252	261	113	,	,	PUNCT
eurjchem-1252	261	114	77	77	NUM
eurjchem-1252	261	115	(	(	PUNCT
eurjchem-1252	261	116	34.97	34.97	NUM
eurjchem-1252	261	117	)	)	PUNCT
eurjchem-1252	261	118	,	,	PUNCT
eurjchem-1252	261	119	76	76	NUM
eurjchem-1252	261	120	(	(	PUNCT
eurjchem-1252	261	121	9.35	9.35	NUM
eurjchem-1252	261	122	)	)	PUNCT
eurjchem-1252	261	123	,	,	PUNCT
eurjchem-1252	261	124	51	51	NUM
eurjchem-1252	261	125	(	(	PUNCT
eurjchem-1252	261	126	34.85	34.85	NUM
eurjchem-1252	261	127	)	)	PUNCT
eurjchem-1252	261	128	.	.	PUNCT
eurjchem-1252	262	1	anal	anal	PROPN
eurjchem-1252	262	2	.	.	PUNCT
eurjchem-1252	262	3	calcd	calcd	NOUN
eurjchem-1252	262	4	.	.	PUNCT
eurjchem-1252	263	1	for	for	ADP
eurjchem-1252	263	2	c28h17n3o4	c28h17n3o4	PROPN
eurjchem-1252	263	3	:	:	PUNCT
eurjchem-1252	263	4	c	c	NOUN
eurjchem-1252	263	5	,	,	PUNCT
eurjchem-1252	263	6	73.20	73.20	NUM
eurjchem-1252	263	7	;	;	PUNCT
eurjchem-1252	263	8	h	h	NOUN
eurjchem-1252	263	9	,	,	PUNCT
eurjchem-1252	263	10	3.73	3.73	NUM
eurjchem-1252	263	11	;	;	PUNCT
eurjchem-1252	263	12	n	n	CCONJ
eurjchem-1252	263	13	,	,	PUNCT
eurjchem-1252	263	14	9.15	9.15	NUM
eurjchem-1252	263	15	.	.	PUNCT
eurjchem-1252	263	16	found	find	VERB
eurjchem-1252	263	17	:	:	PUNCT
eurjchem-1252	264	1	c	c	X
eurjchem-1252	264	2	,	,	PUNCT
eurjchem-1252	264	3	73.48	73.48	NUM
eurjchem-1252	264	4	;	;	PUNCT
eurjchem-1252	264	5	h	h	NOUN
eurjchem-1252	264	6	,	,	PUNCT
eurjchem-1252	264	7	3.62	3.62	NUM
eurjchem-1252	264	8	;	;	PUNCT
eurjchem-1252	264	9	n	n	CCONJ
eurjchem-1252	264	10	,	,	PUNCT
eurjchem-1252	264	11	9.38	9.38	NUM
eurjchem-1252	264	12	%	%	NOUN
eurjchem-1252	264	13	.	.	PUNCT
eurjchem-1252	265	1	2.2.19	2.2.19	NUM
eurjchem-1252	265	2	.	.	PUNCT
eurjchem-1252	266	1	synthesis	synthesis	NOUN
eurjchem-1252	266	2	of	of	ADP
eurjchem-1252	266	3	3‐(hydroxymethylene)‐7,8,9‐triphenyl‐	3‐(hydroxymethylene)‐7,8,9‐triphenyl‐	NUM
eurjchem-1252	266	4	2h‐pyrimido[1,2‐b]pyridazine‐2,4(3h)‐dione	2h‐pyrimido[1,2‐b]pyridazine‐2,4(3h)‐dione	NUM
eurjchem-1252	266	5	(	(	PUNCT
eurjchem-1252	266	6	16	16	NUM
eurjchem-1252	266	7	)	)	PUNCT
eurjchem-1252	266	8	a	a	DET
eurjchem-1252	266	9	solution	solution	NOUN
eurjchem-1252	266	10	of	of	ADP
eurjchem-1252	266	11	compound	compound	NOUN
eurjchem-1252	266	12	1	1	NUM
eurjchem-1252	266	13	(	(	PUNCT
eurjchem-1252	266	14	0.5	0.5	NUM
eurjchem-1252	266	15	g	g	NOUN
eurjchem-1252	266	16	,	,	PUNCT
eurjchem-1252	266	17	1.28	1.28	NUM
eurjchem-1252	266	18	mmol	mmol	NOUN
eurjchem-1252	266	19	)	)	PUNCT
eurjchem-1252	266	20	in	in	ADP
eurjchem-1252	266	21	potassium	potassium	NOUN
eurjchem-1252	266	22	hydroxide	hydroxide	NOUN
eurjchem-1252	266	23	(	(	PUNCT
eurjchem-1252	266	24	10	10	NUM
eurjchem-1252	266	25	ml	ml	NOUN
eurjchem-1252	266	26	,	,	PUNCT
eurjchem-1252	266	27	50	50	NUM
eurjchem-1252	266	28	%	%	NOUN
eurjchem-1252	266	29	)	)	PUNCT
eurjchem-1252	266	30	and	and	CCONJ
eurjchem-1252	266	31	chloroform	chloroform	NOUN
eurjchem-1252	266	32	(	(	PUNCT
eurjchem-1252	266	33	10	10	NUM
eurjchem-1252	266	34	ml	ml	NOUN
eurjchem-1252	266	35	)	)	PUNCT
eurjchem-1252	266	36	was	be	AUX
eurjchem-1252	266	37	refluxed	refluxe	VERB
eurjchem-1252	266	38	for	for	ADP
eurjchem-1252	266	39	12	12	NUM
eurjchem-1252	266	40	h.	h.	NOUN
eurjchem-1252	266	41	the	the	DET
eurjchem-1252	266	42	aq	aq	PROPN
eurjchem-1252	266	43	.	.	PROPN
eurjchem-1252	266	44	layer	layer	NOUN
eurjchem-1252	266	45	was	be	AUX
eurjchem-1252	266	46	separated	separate	VERB
eurjchem-1252	266	47	and	and	CCONJ
eurjchem-1252	266	48	acidified	acidify	VERB
eurjchem-1252	266	49	with	with	ADP
eurjchem-1252	266	50	hydrochloric	hydrochloric	ADJ
eurjchem-1252	266	51	acid	acid	NOUN
eurjchem-1252	266	52	.	.	PUNCT
eurjchem-1252	267	1	the	the	DET
eurjchem-1252	267	2	solid	solid	ADJ
eurjchem-1252	267	3	product	product	NOUN
eurjchem-1252	267	4	formed	form	VERB
eurjchem-1252	267	5	was	be	AUX
eurjchem-1252	267	6	filtered	filter	VERB
eurjchem-1252	267	7	off	off	ADP
eurjchem-1252	267	8	,	,	PUNCT
eurjchem-1252	267	9	washed	wash	VERB
eurjchem-1252	267	10	with	with	ADP
eurjchem-1252	267	11	water	water	NOUN
eurjchem-1252	267	12	,	,	PUNCT
eurjchem-1252	267	13	and	and	CCONJ
eurjchem-1252	267	14	recrystallized	recrystallize	VERB
eurjchem-1252	267	15	from	from	ADP
eurjchem-1252	267	16	chloroform	chloroform	NOUN
eurjchem-1252	267	17	to	to	PART
eurjchem-1252	267	18	give	give	VERB
eurjchem-1252	267	19	compound	compound	NOUN
eurjchem-1252	267	20	16	16	NUM
eurjchem-1252	267	21	as	as	ADP
eurjchem-1252	267	22	pale	pale	ADJ
eurjchem-1252	267	23	brown	brown	ADJ
eurjchem-1252	267	24	crystals	crystal	NOUN
eurjchem-1252	267	25	(	(	PUNCT
eurjchem-1252	267	26	scheme	scheme	NOUN
eurjchem-1252	267	27	3	3	NUM
eurjchem-1252	267	28	)	)	PUNCT
eurjchem-1252	267	29	.	.	PUNCT
eurjchem-1252	268	1	color	color	NOUN
eurjchem-1252	268	2	:	:	PUNCT
eurjchem-1252	268	3	pale	pale	ADJ
eurjchem-1252	268	4	brown	brown	NOUN
eurjchem-1252	268	5	.	.	PUNCT
eurjchem-1252	269	1	yield	yield	NOUN
eurjchem-1252	269	2	:	:	PUNCT
eurjchem-1252	269	3	70.92	70.92	NUM
eurjchem-1252	269	4	%	%	NOUN
eurjchem-1252	269	5	.	.	PUNCT
eurjchem-1252	270	1	m.p	m.p	PROPN
eurjchem-1252	270	2	.	.	PROPN
eurjchem-1252	270	3	:	:	PUNCT
eurjchem-1252	271	1	143‐145	143‐145	PROPN
eurjchem-1252	271	2	°	°	ADP
eurjchem-1252	271	3	c	c	X
eurjchem-1252	271	4	.	.	PUNCT
eurjchem-1252	272	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	272	2	(	(	PUNCT
eurjchem-1252	272	3	kbr	kbr	PROPN
eurjchem-1252	272	4	,	,	PUNCT
eurjchem-1252	272	5	ν	ν	PROPN
eurjchem-1252	272	6	,	,	PUNCT
eurjchem-1252	272	7	cm‐	cm‐	NOUN
eurjchem-1252	272	8	1	1	NUM
eurjchem-1252	272	9	):	):	PUNCT
eurjchem-1252	272	10	3423	3423	NUM
eurjchem-1252	272	11	(	(	PUNCT
eurjchem-1252	272	12	oh	oh	INTJ
eurjchem-1252	272	13	)	)	PUNCT
eurjchem-1252	272	14	,	,	PUNCT
eurjchem-1252	272	15	3057	3057	NUM
eurjchem-1252	272	16	(	(	PUNCT
eurjchem-1252	272	17	ch	ch	NOUN
eurjchem-1252	272	18	,	,	PUNCT
eurjchem-1252	272	19	arom	arom	NOUN
eurjchem-1252	272	20	.	.	PUNCT
eurjchem-1252	272	21	)	)	PUNCT
eurjchem-1252	272	22	,	,	PUNCT
eurjchem-1252	272	23	1714	1714	NUM
eurjchem-1252	272	24	(	(	PUNCT
eurjchem-1252	272	25	c	c	NOUN
eurjchem-1252	272	26	=	=	NOUN
eurjchem-1252	272	27	o	o	NOUN
eurjchem-1252	272	28	)	)	PUNCT
eurjchem-1252	272	29	,	,	PUNCT
eurjchem-1252	272	30	1635	1635	NUM
eurjchem-1252	272	31	(	(	PUNCT
eurjchem-1252	272	32	c	c	NOUN
eurjchem-1252	272	33	=	=	SYM
eurjchem-1252	272	34	n	n	NUM
eurjchem-1252	272	35	)	)	PUNCT
eurjchem-1252	272	36	.	.	PUNCT
eurjchem-1252	273	1	ms	ms	NOUN
eurjchem-1252	273	2	(	(	PUNCT
eurjchem-1252	273	3	ei	ei	PROPN
eurjchem-1252	273	4	,	,	PUNCT
eurjchem-1252	273	5	m	m	PROPN
eurjchem-1252	273	6	/	/	SYM
eurjchem-1252	273	7	z	z	PROPN
eurjchem-1252	273	8	(	(	PUNCT
eurjchem-1252	273	9	%	%	NOUN
eurjchem-1252	273	10	)	)	PUNCT
eurjchem-1252	273	11	):	):	PUNCT
eurjchem-1252	273	12	420	420	NUM
eurjchem-1252	273	13	(	(	PUNCT
eurjchem-1252	273	14	m+	m+	NUM
eurjchem-1252	273	15	,	,	PUNCT
eurjchem-1252	273	16	8.23	8.23	NUM
eurjchem-1252	273	17	)	)	PUNCT
eurjchem-1252	273	18	,	,	PUNCT
eurjchem-1252	273	19	402	402	NUM
eurjchem-1252	273	20	(	(	PUNCT
eurjchem-1252	273	21	6.96	6.96	NUM
eurjchem-1252	273	22	)	)	PUNCT
eurjchem-1252	273	23	,	,	PUNCT
eurjchem-1252	273	24	391	391	NUM
eurjchem-1252	273	25	(	(	PUNCT
eurjchem-1252	273	26	6.58	6.58	NUM
eurjchem-1252	273	27	)	)	PUNCT
eurjchem-1252	273	28	,	,	PUNCT
eurjchem-1252	273	29	350	350	NUM
eurjchem-1252	273	30	(	(	PUNCT
eurjchem-1252	273	31	7.97	7.97	NUM
eurjchem-1252	273	32	)	)	PUNCT
eurjchem-1252	273	33	,	,	PUNCT
eurjchem-1252	273	34	337	337	NUM
eurjchem-1252	273	35	(	(	PUNCT
eurjchem-1252	273	36	8.86	8.86	NUM
eurjchem-1252	273	37	)	)	PUNCT
eurjchem-1252	273	38	,	,	PUNCT
eurjchem-1252	273	39	277	277	NUM
eurjchem-1252	273	40	(	(	PUNCT
eurjchem-1252	273	41	100	100	NUM
eurjchem-1252	273	42	)	)	PUNCT
eurjchem-1252	273	43	,	,	PUNCT
eurjchem-1252	273	44	267	267	NUM
eurjchem-1252	273	45	(	(	PUNCT
eurjchem-1252	273	46	7.59	7.59	NUM
eurjchem-1252	273	47	)	)	PUNCT
eurjchem-1252	273	48	,	,	PUNCT
eurjchem-1252	273	49	191	191	NUM
eurjchem-1252	273	50	(	(	PUNCT
eurjchem-1252	273	51	6.58	6.58	NUM
eurjchem-1252	273	52	)	)	PUNCT
eurjchem-1252	273	53	,	,	PUNCT
eurjchem-1252	273	54	152	152	NUM
eurjchem-1252	273	55	(	(	PUNCT
eurjchem-1252	273	56	8.99	8.99	NUM
eurjchem-1252	273	57	)	)	PUNCT
eurjchem-1252	273	58	,	,	PUNCT
eurjchem-1252	273	59	143	143	NUM
eurjchem-1252	273	60	(	(	PUNCT
eurjchem-1252	273	61	6.84	6.84	NUM
eurjchem-1252	273	62	)	)	PUNCT
eurjchem-1252	273	63	,	,	PUNCT
eurjchem-1252	273	64	82	82	NUM
eurjchem-1252	273	65	(	(	PUNCT
eurjchem-1252	273	66	6.84	6.84	NUM
eurjchem-1252	273	67	)	)	PUNCT
eurjchem-1252	273	68	,	,	PUNCT
eurjchem-1252	273	69	76	76	NUM
eurjchem-1252	273	70	(	(	PUNCT
eurjchem-1252	273	71	8.23	8.23	NUM
eurjchem-1252	273	72	)	)	PUNCT
eurjchem-1252	273	73	,	,	PUNCT
eurjchem-1252	273	74	69	69	NUM
eurjchem-1252	273	75	(	(	PUNCT
eurjchem-1252	273	76	11.39	11.39	NUM
eurjchem-1252	273	77	)	)	PUNCT
eurjchem-1252	273	78	.	.	PUNCT
eurjchem-1252	274	1	anal	anal	PROPN
eurjchem-1252	274	2	.	.	PUNCT
eurjchem-1252	274	3	calcd	calcd	NOUN
eurjchem-1252	274	4	.	.	PUNCT
eurjchem-1252	275	1	for	for	ADP
eurjchem-1252	275	2	c26h17n3o3	c26h17n3o3	NOUN
eurjchem-1252	275	3	:	:	PUNCT
eurjchem-1252	275	4	c	c	X
eurjchem-1252	275	5	,	,	PUNCT
eurjchem-1252	275	6	74.45	74.45	NUM
eurjchem-1252	275	7	;	;	PUNCT
eurjchem-1252	275	8	h	h	NOUN
eurjchem-1252	275	9	,	,	PUNCT
eurjchem-1252	275	10	4.09	4.09	NUM
eurjchem-1252	275	11	;	;	PUNCT
eurjchem-1252	275	12	n	n	CCONJ
eurjchem-1252	275	13	,	,	PUNCT
eurjchem-1252	275	14	10.02	10.02	NUM
eurjchem-1252	275	15	.	.	PUNCT
eurjchem-1252	275	16	found	find	VERB
eurjchem-1252	275	17	:	:	PUNCT
eurjchem-1252	276	1	c	c	X
eurjchem-1252	276	2	,	,	PUNCT
eurjchem-1252	276	3	74.63	74.63	NUM
eurjchem-1252	276	4	;	;	PUNCT
eurjchem-1252	276	5	h	h	NOUN
eurjchem-1252	276	6	,	,	PUNCT
eurjchem-1252	276	7	4.17	4.17	NUM
eurjchem-1252	276	8	;	;	PUNCT
eurjchem-1252	276	9	n	n	CCONJ
eurjchem-1252	276	10	,	,	PUNCT
eurjchem-1252	276	11	10.18	10.18	NUM
eurjchem-1252	276	12	%	%	NOUN
eurjchem-1252	276	13	.	.	PUNCT
eurjchem-1252	277	1	2.2.20	2.2.20	NUM
eurjchem-1252	277	2	.	.	PUNCT
eurjchem-1252	277	3	synthesis	synthesis	NOUN
eurjchem-1252	277	4	of	of	ADP
eurjchem-1252	277	5	2‐chloro‐4‐oxo‐7,8,9‐triphenyl‐4h‐	2‐chloro‐4‐oxo‐7,8,9‐triphenyl‐4h‐	DET
eurjchem-1252	277	6	pyrimido[1,2‐b]pyridazine‐3‐carbaldehyde	pyrimido[1,2‐b]pyridazine‐3‐carbaldehyde	X
eurjchem-1252	277	7	(	(	PUNCT
eurjchem-1252	277	8	17	17	NUM
eurjchem-1252	277	9	)	)	PUNCT
eurjchem-1252	277	10	method	method	NOUN
eurjchem-1252	277	11	a	a	DET
eurjchem-1252	277	12	:	:	PUNCT
eurjchem-1252	277	13	a	a	DET
eurjchem-1252	277	14	solution	solution	NOUN
eurjchem-1252	277	15	of	of	ADP
eurjchem-1252	277	16	compound	compound	NOUN
eurjchem-1252	277	17	1	1	NUM
eurjchem-1252	277	18	(	(	PUNCT
eurjchem-1252	277	19	0.5	0.5	NUM
eurjchem-1252	277	20	g	g	NOUN
eurjchem-1252	277	21	,	,	PUNCT
eurjchem-1252	277	22	1.28	1.28	NUM
eurjchem-1252	277	23	mmol	mmol	NOUN
eurjchem-1252	277	24	)	)	PUNCT
eurjchem-1252	277	25	in	in	ADP
eurjchem-1252	277	26	dimethylformamide	dimethylformamide	NOUN
eurjchem-1252	277	27	(	(	PUNCT
eurjchem-1252	277	28	10	10	NUM
eurjchem-1252	277	29	ml	ml	NOUN
eurjchem-1252	277	30	)	)	PUNCT
eurjchem-1252	277	31	and	and	CCONJ
eurjchem-1252	277	32	phosphoryl	phosphoryl	PROPN
eurjchem-1252	277	33	chloride	chloride	PROPN
eurjchem-1252	277	34	(	(	PUNCT
eurjchem-1252	277	35	2	2	NUM
eurjchem-1252	277	36	ml	ml	NOUN
eurjchem-1252	277	37	)	)	PUNCT
eurjchem-1252	277	38	was	be	AUX
eurjchem-1252	277	39	stirred	stir	VERB
eurjchem-1252	277	40	at	at	ADP
eurjchem-1252	277	41	60	60	NUM
eurjchem-1252	277	42	°	°	ADP
eurjchem-1252	277	43	c	c	NOUN
eurjchem-1252	277	44	for	for	ADP
eurjchem-1252	277	45	2	2	NUM
eurjchem-1252	277	46	h	h	NOUN
eurjchem-1252	277	47	,	,	PUNCT
eurjchem-1252	277	48	then	then	ADV
eurjchem-1252	277	49	the	the	DET
eurjchem-1252	277	50	reaction	reaction	NOUN
eurjchem-1252	277	51	mixture	mixture	NOUN
eurjchem-1252	277	52	was	be	AUX
eurjchem-1252	277	53	cooled	cool	VERB
eurjchem-1252	277	54	,	,	PUNCT
eurjchem-1252	277	55	and	and	CCONJ
eurjchem-1252	277	56	poured	pour	VERB
eurjchem-1252	277	57	into	into	ADP
eurjchem-1252	277	58	ice	ice	NOUN
eurjchem-1252	277	59	cold	cold	ADJ
eurjchem-1252	277	60	water	water	NOUN
eurjchem-1252	277	61	(	(	PUNCT
eurjchem-1252	277	62	200	200	NUM
eurjchem-1252	277	63	ml	ml	NOUN
eurjchem-1252	277	64	)	)	PUNCT
eurjchem-1252	277	65	.	.	PUNCT
eurjchem-1252	278	1	the	the	DET
eurjchem-1252	278	2	precipitate	precipitate	NOUN
eurjchem-1252	278	3	was	be	AUX
eurjchem-1252	278	4	filtered	filter	VERB
eurjchem-1252	278	5	off	off	ADP
eurjchem-1252	278	6	,	,	PUNCT
eurjchem-1252	278	7	washed	wash	VERB
eurjchem-1252	278	8	with	with	ADP
eurjchem-1252	278	9	water	water	NOUN
eurjchem-1252	278	10	,	,	PUNCT
eurjchem-1252	278	11	dried	dry	VERB
eurjchem-1252	278	12	,	,	PUNCT
eurjchem-1252	278	13	and	and	CCONJ
eurjchem-1252	278	14	recrystallized	recrystallize	VERB
eurjchem-1252	278	15	from	from	ADP
eurjchem-1252	278	16	acetone	acetone	NOUN
eurjchem-1252	278	17	to	to	PART
eurjchem-1252	278	18	give	give	VERB
eurjchem-1252	278	19	compound	compound	NOUN
eurjchem-1252	278	20	17	17	NUM
eurjchem-1252	278	21	(	(	PUNCT
eurjchem-1252	278	22	scheme	scheme	NOUN
eurjchem-1252	278	23	3	3	NUM
eurjchem-1252	278	24	)	)	PUNCT
eurjchem-1252	278	25	.	.	PUNCT
eurjchem-1252	279	1	color	color	NOUN
eurjchem-1252	279	2	:	:	PUNCT
eurjchem-1252	279	3	dark	dark	PROPN
eurjchem-1252	279	4	brown	brown	PROPN
eurjchem-1252	279	5	.	.	PUNCT
eurjchem-1252	280	1	yield	yield	NOUN
eurjchem-1252	280	2	:	:	PUNCT
eurjchem-1252	280	3	69.73	69.73	NUM
eurjchem-1252	280	4	%	%	NOUN
eurjchem-1252	280	5	.	.	PUNCT
eurjchem-1252	281	1	m.p	m.p	PROPN
eurjchem-1252	281	2	.	.	PROPN
eurjchem-1252	281	3	:	:	PUNCT
eurjchem-1252	282	1	179‐180	179‐180	NUM
eurjchem-1252	282	2	°	°	PROPN
eurjchem-1252	282	3	c	c	X
eurjchem-1252	282	4	.	.	PUNCT
eurjchem-1252	283	1	ft‐ir	ft‐ir	NOUN
eurjchem-1252	283	2	(	(	PUNCT
eurjchem-1252	283	3	kbr	kbr	PROPN
eurjchem-1252	283	4	,	,	PUNCT
eurjchem-1252	283	5	ν	ν	PROPN
eurjchem-1252	283	6	,	,	PUNCT
eurjchem-1252	283	7	cm‐1	cm‐1	PROPN
eurjchem-1252	283	8	):	):	PUNCT
eurjchem-1252	283	9	3057	3057	NUM
eurjchem-1252	283	10	(	(	PUNCT
eurjchem-1252	283	11	ch	ch	NOUN
eurjchem-1252	283	12	,	,	PUNCT
eurjchem-1252	283	13	arom	arom	NOUN
eurjchem-1252	283	14	.	.	PUNCT
eurjchem-1252	283	15	)	)	PUNCT
eurjchem-1252	283	16	,	,	PUNCT
eurjchem-1252	283	17	2925	2925	NUM
eurjchem-1252	283	18	,	,	PUNCT
eurjchem-1252	283	19	2854	2854	NUM
eurjchem-1252	283	20	(	(	PUNCT
eurjchem-1252	283	21	ch	ch	NOUN
eurjchem-1252	283	22	aliph	aliph	PROPN
eurjchem-1252	283	23	.	.	PUNCT
eurjchem-1252	283	24	)	)	PUNCT
eurjchem-1252	283	25	,	,	PUNCT
eurjchem-1252	283	26	1714	1714	NUM
eurjchem-1252	283	27	(	(	PUNCT
eurjchem-1252	283	28	c	c	NOUN
eurjchem-1252	283	29	=	=	NOUN
eurjchem-1252	283	30	o	o	NOUN
eurjchem-1252	283	31	)	)	PUNCT
eurjchem-1252	283	32	,	,	PUNCT
eurjchem-1252	283	33	1635	1635	NUM
eurjchem-1252	283	34	(	(	PUNCT
eurjchem-1252	283	35	c	c	NOUN
eurjchem-1252	283	36	=	=	SYM
eurjchem-1252	283	37	n	n	NUM
eurjchem-1252	283	38	)	)	PUNCT
eurjchem-1252	283	39	.	.	PUNCT
eurjchem-1252	284	1	1h	1h	NUM
eurjchem-1252	284	2	nmr	nmr	NOUN
eurjchem-1252	284	3	(	(	PUNCT
eurjchem-1252	284	4	300	300	NUM
eurjchem-1252	284	5	mhz	mhz	NOUN
eurjchem-1252	284	6	,	,	PUNCT
eurjchem-1252	284	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1252	284	8	,	,	PUNCT
eurjchem-1252	284	9	δ	δ	PROPN
eurjchem-1252	284	10	,	,	PUNCT
eurjchem-1252	284	11	ppm	ppm	NUM
eurjchem-1252	284	12	):	):	PUNCT
eurjchem-1252	284	13	6.60‐7.66	6.60‐7.66	NUM
eurjchem-1252	284	14	(	(	PUNCT
eurjchem-1252	284	15	m	m	PROPN
eurjchem-1252	284	16	,	,	PUNCT
eurjchem-1252	284	17	15h	15h	NUM
eurjchem-1252	284	18	,	,	PUNCT
eurjchem-1252	284	19	3ph	3ph	NOUN
eurjchem-1252	284	20	)	)	PUNCT
eurjchem-1252	284	21	,	,	PUNCT
eurjchem-1252	284	22	10.22	10.22	NUM
eurjchem-1252	284	23	(	(	PUNCT
eurjchem-1252	284	24	s	s	PROPN
eurjchem-1252	284	25	,	,	PUNCT
eurjchem-1252	284	26	1h	1h	NUM
eurjchem-1252	284	27	,	,	PUNCT
eurjchem-1252	284	28	cho	cho	NOUN
eurjchem-1252	284	29	)	)	PUNCT
eurjchem-1252	284	30	.	.	PUNCT
eurjchem-1252	285	1	ms	ms	NOUN
eurjchem-1252	285	2	(	(	PUNCT
eurjchem-1252	285	3	ei	ei	PROPN
eurjchem-1252	285	4	,	,	PUNCT
eurjchem-1252	285	5	m	m	PROPN
eurjchem-1252	285	6	/	/	SYM
eurjchem-1252	285	7	z	z	PROPN
eurjchem-1252	285	8	(	(	PUNCT
eurjchem-1252	285	9	%	%	NOUN
eurjchem-1252	285	10	)	)	PUNCT
eurjchem-1252	285	11	):	):	PUNCT
eurjchem-1252	285	12	440	440	NUM
eurjchem-1252	285	13	(	(	PUNCT
eurjchem-1252	285	14	m+	m+	NOUN
eurjchem-1252	285	15	+2	+2	NOUN
eurjchem-1252	285	16	,	,	PUNCT
eurjchem-1252	285	17	0.2	0.2	NUM
eurjchem-1252	285	18	)	)	PUNCT
eurjchem-1252	285	19	,	,	PUNCT
eurjchem-1252	285	20	438	438	NUM
eurjchem-1252	285	21	(	(	PUNCT
eurjchem-1252	285	22	m+	m+	NUM
eurjchem-1252	285	23	,	,	PUNCT
eurjchem-1252	285	24	10.96	10.96	NUM
eurjchem-1252	285	25	)	)	PUNCT
eurjchem-1252	285	26	,	,	PUNCT
eurjchem-1252	285	27	410	410	NUM
eurjchem-1252	285	28	(	(	PUNCT
eurjchem-1252	285	29	9.31	9.31	NUM
eurjchem-1252	285	30	)	)	PUNCT
eurjchem-1252	285	31	,	,	PUNCT
eurjchem-1252	285	32	409	409	NUM
eurjchem-1252	285	33	(	(	PUNCT
eurjchem-1252	285	34	9.76	9.76	NUM
eurjchem-1252	285	35	)	)	PUNCT
eurjchem-1252	285	36	,	,	PUNCT
eurjchem-1252	285	37	401	401	NUM
eurjchem-1252	285	38	(	(	PUNCT
eurjchem-1252	285	39	7.81	7.81	NUM
eurjchem-1252	285	40	)	)	PUNCT
eurjchem-1252	285	41	,	,	PUNCT
eurjchem-1252	285	42	397	397	NUM
eurjchem-1252	285	43	(	(	PUNCT
eurjchem-1252	285	44	8.71	8.71	NUM
eurjchem-1252	285	45	)	)	PUNCT
eurjchem-1252	285	46	,	,	PUNCT
eurjchem-1252	285	47	361	361	NUM
eurjchem-1252	285	48	(	(	PUNCT
eurjchem-1252	285	49	11.41	11.41	NUM
eurjchem-1252	285	50	)	)	PUNCT
eurjchem-1252	285	51	,	,	PUNCT
eurjchem-1252	285	52	348	348	NUM
eurjchem-1252	285	53	(	(	PUNCT
eurjchem-1252	285	54	9.01	9.01	NUM
eurjchem-1252	285	55	)	)	PUNCT
eurjchem-1252	285	56	,	,	PUNCT
eurjchem-1252	285	57	333	333	NUM
eurjchem-1252	285	58	(	(	PUNCT
eurjchem-1252	285	59	11.11	11.11	NUM
eurjchem-1252	285	60	)	)	PUNCT
eurjchem-1252	285	61	,	,	PUNCT
eurjchem-1252	285	62	277	277	NUM
eurjchem-1252	285	63	(	(	PUNCT
eurjchem-1252	285	64	40.54	40.54	NUM
eurjchem-1252	285	65	)	)	PUNCT
eurjchem-1252	285	66	,	,	PUNCT
eurjchem-1252	285	67	161	161	NUM
eurjchem-1252	285	68	(	(	PUNCT
eurjchem-1252	285	69	8.11	8.11	NUM
eurjchem-1252	285	70	)	)	PUNCT
eurjchem-1252	285	71	,	,	PUNCT
eurjchem-1252	285	72	104	104	NUM
eurjchem-1252	285	73	(	(	PUNCT
eurjchem-1252	285	74	10.51	10.51	NUM
eurjchem-1252	285	75	)	)	PUNCT
eurjchem-1252	285	76	,	,	PUNCT
eurjchem-1252	285	77	89	89	NUM
eurjchem-1252	285	78	(	(	PUNCT
eurjchem-1252	285	79	12.31	12.31	NUM
eurjchem-1252	285	80	)	)	PUNCT
eurjchem-1252	285	81	,	,	PUNCT
eurjchem-1252	285	82	77	77	NUM
eurjchem-1252	285	83	(	(	PUNCT
eurjchem-1252	285	84	25.83	25.83	NUM
eurjchem-1252	285	85	)	)	PUNCT
eurjchem-1252	285	86	,	,	PUNCT
eurjchem-1252	285	87	64	64	NUM
eurjchem-1252	285	88	(	(	PUNCT
eurjchem-1252	285	89	100	100	NUM
eurjchem-1252	285	90	)	)	PUNCT
eurjchem-1252	285	91	.	.	PUNCT
eurjchem-1252	286	1	anal	anal	PROPN
eurjchem-1252	286	2	.	.	PUNCT
eurjchem-1252	286	3	calcd	calcd	NOUN
eurjchem-1252	286	4	.	.	PUNCT
eurjchem-1252	287	1	for	for	ADP
eurjchem-1252	287	2	c26h16cln3o2	c26h16cln3o2	NOUN
eurjchem-1252	287	3	:	:	PUNCT
eurjchem-1252	287	4	c	c	X
eurjchem-1252	287	5	,	,	PUNCT
eurjchem-1252	287	6	71.31	71.31	NUM
eurjchem-1252	287	7	;	;	PUNCT
eurjchem-1252	287	8	h	h	NOUN
eurjchem-1252	287	9	,	,	PUNCT
eurjchem-1252	287	10	3.68	3.68	NUM
eurjchem-1252	287	11	;	;	PUNCT
eurjchem-1252	287	12	n	n	CCONJ
eurjchem-1252	287	13	,	,	PUNCT
eurjchem-1252	287	14	9.60	9.60	NUM
eurjchem-1252	287	15	.	.	PUNCT
eurjchem-1252	287	16	found	find	VERB
eurjchem-1252	287	17	:	:	PUNCT
eurjchem-1252	288	1	c	c	X
eurjchem-1252	288	2	,	,	PUNCT
eurjchem-1252	288	3	71.69	71.69	NUM
eurjchem-1252	288	4	;	;	PUNCT
eurjchem-1252	288	5	h	h	NOUN
eurjchem-1252	288	6	,	,	PUNCT
eurjchem-1252	288	7	3.76	3.76	NUM
eurjchem-1252	288	8	;	;	PUNCT
eurjchem-1252	288	9	n	n	CCONJ
eurjchem-1252	288	10	,	,	PUNCT
eurjchem-1252	288	11	9.74	9.74	NUM
eurjchem-1252	288	12	%	%	NOUN
eurjchem-1252	288	13	.	.	PUNCT
eurjchem-1252	289	1	method	method	PROPN
eurjchem-1252	289	2	b	b	NOUN
eurjchem-1252	289	3	:	:	PUNCT
eurjchem-1252	289	4	a	a	DET
eurjchem-1252	289	5	mixture	mixture	NOUN
eurjchem-1252	289	6	of	of	ADP
eurjchem-1252	289	7	compound	compound	NOUN
eurjchem-1252	289	8	16	16	NUM
eurjchem-1252	289	9	(	(	PUNCT
eurjchem-1252	289	10	0.5	0.5	NUM
eurjchem-1252	289	11	g	g	NOUN
eurjchem-1252	289	12	,	,	PUNCT
eurjchem-1252	289	13	1.19	1.19	NUM
eurjchem-1252	289	14	mmol	mmol	NOUN
eurjchem-1252	289	15	)	)	PUNCT
eurjchem-1252	289	16	and	and	CCONJ
eurjchem-1252	289	17	phosphoryl	phosphoryl	PROPN
eurjchem-1252	289	18	chloride	chloride	PROPN
eurjchem-1252	289	19	(	(	PUNCT
eurjchem-1252	289	20	10	10	NUM
eurjchem-1252	289	21	ml	ml	NOUN
eurjchem-1252	289	22	)	)	PUNCT
eurjchem-1252	289	23	was	be	AUX
eurjchem-1252	289	24	refluxed	refluxe	VERB
eurjchem-1252	289	25	for	for	ADP
eurjchem-1252	289	26	1	1	NUM
eurjchem-1252	289	27	h.	h.	NOUN
eurjchem-1252	289	28	the	the	DET
eurjchem-1252	289	29	reaction	reaction	NOUN
eurjchem-1252	289	30	mixture	mixture	NOUN
eurjchem-1252	289	31	was	be	AUX
eurjchem-1252	289	32	cooled	cool	VERB
eurjchem-1252	289	33	,	,	PUNCT
eurjchem-1252	289	34	and	and	CCONJ
eurjchem-1252	289	35	poured	pour	VERB
eurjchem-1252	289	36	into	into	ADP
eurjchem-1252	289	37	ice	ice	NOUN
eurjchem-1252	289	38	cold	cold	ADJ
eurjchem-1252	289	39	water	water	NOUN
eurjchem-1252	289	40	(	(	PUNCT
eurjchem-1252	289	41	200	200	NUM
eurjchem-1252	289	42	ml	ml	NOUN
eurjchem-1252	289	43	)	)	PUNCT
eurjchem-1252	289	44	.	.	PUNCT
eurjchem-1252	290	1	the	the	DET
eurjchem-1252	290	2	solid	solid	ADJ
eurjchem-1252	290	3	product	product	NOUN
eurjchem-1252	290	4	was	be	AUX
eurjchem-1252	290	5	filtered	filter	VERB
eurjchem-1252	290	6	off	off	ADP
eurjchem-1252	290	7	,	,	PUNCT
eurjchem-1252	290	8	washed	wash	VERB
eurjchem-1252	290	9	with	with	ADP
eurjchem-1252	290	10	water	water	NOUN
eurjchem-1252	290	11	,	,	PUNCT
eurjchem-1252	290	12	dried	dry	VERB
eurjchem-1252	290	13	,	,	PUNCT
eurjchem-1252	290	14	and	and	CCONJ
eurjchem-1252	290	15	recrystallized	recrystallize	VERB
eurjchem-1252	290	16	from	from	ADP
eurjchem-1252	290	17	acetone	acetone	NOUN
eurjchem-1252	290	18	to	to	PART
eurjchem-1252	290	19	give	give	VERB
eurjchem-1252	290	20	compound	compound	NOUN
eurjchem-1252	290	21	17	17	NUM
eurjchem-1252	290	22	as	as	ADP
eurjchem-1252	290	23	dark	dark	ADJ
eurjchem-1252	290	24	brown	brown	ADJ
eurjchem-1252	290	25	crystals	crystal	NOUN
eurjchem-1252	290	26	.	.	PUNCT
eurjchem-1252	291	1	2.2.21	2.2.21	NUM
eurjchem-1252	291	2	.	.	PUNCT
eurjchem-1252	291	3	measuring	measure	VERB
eurjchem-1252	291	4	the	the	DET
eurjchem-1252	291	5	antimicrobial	antimicrobial	ADJ
eurjchem-1252	291	6	activity	activity	NOUN
eurjchem-1252	291	7	of	of	ADP
eurjchem-1252	291	8	compounds	compound	NOUN
eurjchem-1252	291	9	(	(	PUNCT
eurjchem-1252	291	10	2‐17	2‐17	NUM
eurjchem-1252	291	11	)	)	PUNCT
eurjchem-1252	291	12	applying	apply	VERB
eurjchem-1252	291	13	the	the	DET
eurjchem-1252	291	14	agar	agar	NOUN
eurjchem-1252	291	15	plate	plate	NOUN
eurjchem-1252	291	16	diffusion	diffusion	NOUN
eurjchem-1252	291	17	technique	technique	NOUN
eurjchem-1252	291	18	[	[	X
eurjchem-1252	291	19	7	7	NUM
eurjchem-1252	291	20	]	]	PUNCT
eurjchem-1252	291	21	,	,	PUNCT
eurjchem-1252	291	22	the	the	DET
eurjchem-1252	291	23	newly	newly	ADV
eurjchem-1252	291	24	synthesised	synthesise	VERB
eurjchem-1252	291	25	compounds	compound	NOUN
eurjchem-1252	291	26	were	be	AUX
eurjchem-1252	291	27	screened	screen	VERB
eurjchem-1252	291	28	for	for	ADP
eurjchem-1252	291	29	their	their	PRON
eurjchem-1252	291	30	antimicrobial	antimicrobial	ADJ
eurjchem-1252	291	31	activity	activity	NOUN
eurjchem-1252	291	32	against	against	ADP
eurjchem-1252	291	33	gram	gram	NOUN
eurjchem-1252	291	34	positive	positive	ADJ
eurjchem-1252	291	35	bacteria	bacteria	NOUN
eurjchem-1252	291	36	(	(	PUNCT
eurjchem-1252	291	37	staphylococcus	staphylococcus	NOUN
eurjchem-1252	291	38	aureus	aureus	NOUN
eurjchem-1252	291	39	)	)	PUNCT
eurjchem-1252	291	40	,	,	PUNCT
eurjchem-1252	291	41	gram	gram	PROPN
eurjchem-1252	291	42	negative	negative	ADJ
eurjchem-1252	291	43	bacteria	bacteria	NOUN
eurjchem-1252	291	44	(	(	PUNCT
eurjchem-1252	291	45	escherichia	escherichia	NOUN
eurjchem-1252	291	46	coli	coli	NOUN
eurjchem-1252	291	47	)	)	PUNCT
eurjchem-1252	291	48	,	,	PUNCT
eurjchem-1252	291	49	yeast	yeast	NOUN
eurjchem-1252	291	50	(	(	PUNCT
eurjchem-1252	291	51	candida	candida	PROPN
eurjchem-1252	291	52	albican	albican	PROPN
eurjchem-1252	291	53	)	)	PUNCT
eurjchem-1252	291	54	,	,	PUNCT
eurjchem-1252	291	55	and	and	CCONJ
eurjchem-1252	291	56	fungi	fungus	NOUN
eurjchem-1252	291	57	(	(	PUNCT
eurjchem-1252	291	58	aspergillus	aspergillus	NOUN
eurjchem-1252	291	59	flavus	flavus	NOUN
eurjchem-1252	291	60	)	)	PUNCT
eurjchem-1252	291	61	.	.	PUNCT
eurjchem-1252	292	1	briefly	briefly	NOUN
eurjchem-1252	292	2	,	,	PUNCT
eurjchem-1252	292	3	100	100	NUM
eurjchem-1252	292	4	μl	μl	ADP
eurjchem-1252	292	5	of	of	ADP
eurjchem-1252	292	6	the	the	DET
eurjchem-1252	292	7	tested	test	VERB
eurjchem-1252	292	8	bacteria	bacteria	NOUN
eurjchem-1252	292	9	/	/	SYM
eurjchem-1252	292	10	fungi	fungus	NOUN
eurjchem-1252	292	11	were	be	AUX
eurjchem-1252	292	12	grown	grow	VERB
eurjchem-1252	292	13	in	in	ADP
eurjchem-1252	292	14	10	10	NUM
eurjchem-1252	292	15	ml	ml	NOUN
eurjchem-1252	292	16	of	of	ADP
eurjchem-1252	292	17	fresh	fresh	ADJ
eurjchem-1252	292	18	media	medium	NOUN
eurjchem-1252	292	19	until	until	SCONJ
eurjchem-1252	292	20	they	they	PRON
eurjchem-1252	292	21	reached	reach	VERB
eurjchem-1252	292	22	a	a	DET
eurjchem-1252	292	23	count	count	NOUN
eurjchem-1252	292	24	of	of	ADP
eurjchem-1252	292	25	approximately	approximately	ADV
eurjchem-1252	292	26	108	108	NUM
eurjchem-1252	292	27	cells	cell	NOUN
eurjchem-1252	292	28	/	/	SYM
eurjchem-1252	292	29	ml	ml	X
eurjchem-1252	292	30	for	for	ADP
eurjchem-1252	292	31	bacteria	bacteria	NOUN
eurjchem-1252	292	32	or	or	CCONJ
eurjchem-1252	292	33	105	105	NUM
eurjchem-1252	292	34	cells	cell	NOUN
eurjchem-1252	292	35	/	/	SYM
eurjchem-1252	292	36	ml	ml	X
eurjchem-1252	292	37	for	for	ADP
eurjchem-1252	292	38	fungi	fungus	NOUN
eurjchem-1252	292	39	[	[	X
eurjchem-1252	292	40	8	8	NUM
eurjchem-1252	292	41	]	]	PUNCT
eurjchem-1252	292	42	,	,	PUNCT
eurjchem-1252	292	43	100	100	NUM
eurjchem-1252	292	44	μl	μl	ADP
eurjchem-1252	292	45	of	of	ADP
eurjchem-1252	292	46	microbial	microbial	ADJ
eurjchem-1252	292	47	suspension	suspension	NOUN
eurjchem-1252	292	48	was	be	AUX
eurjchem-1252	292	49	spread	spread	VERB
eurjchem-1252	292	50	onto	onto	ADP
eurjchem-1252	292	51	agar	agar	NOUN
eurjchem-1252	292	52	plates	plate	NOUN
eurjchem-1252	292	53	correspon‐	correspon‐	VERB
eurjchem-1252	292	54	ding	de	VERB
eurjchem-1252	292	55	to	to	ADP
eurjchem-1252	292	56	the	the	DET
eurjchem-1252	292	57	broth	broth	NOUN
eurjchem-1252	292	58	in	in	ADP
eurjchem-1252	292	59	which	which	PRON
eurjchem-1252	292	60	they	they	PRON
eurjchem-1252	292	61	were	be	AUX
eurjchem-1252	292	62	maintained	maintain	VERB
eurjchem-1252	292	63	.	.	PUNCT
eurjchem-1252	293	1	the	the	DET
eurjchem-1252	293	2	plates	plate	NOUN
eurjchem-1252	293	3	inoculated	inoculate	VERB
eurjchem-1252	293	4	with	with	ADP
eurjchem-1252	293	5	filamentous	filamentous	ADJ
eurjchem-1252	293	6	fungi	fungus	NOUN
eurjchem-1252	293	7	were	be	AUX
eurjchem-1252	293	8	incubated	incubate	VERB
eurjchem-1252	293	9	at	at	ADP
eurjchem-1252	293	10	25	25	NUM
eurjchem-1252	293	11	°	°	NOUN
eurjchem-1252	293	12	c	c	NOUN
eurjchem-1252	293	13	for	for	ADP
eurjchem-1252	293	14	48	48	NUM
eurjchem-1252	293	15	h	h	NOUN
eurjchem-1252	293	16	,	,	PUNCT
eurjchem-1252	293	17	bacteria	bacteria	NOUN
eurjchem-1252	293	18	at	at	ADP
eurjchem-1252	293	19	35‐37	35‐37	NUM
eurjchem-1252	293	20	°	°	ADP
eurjchem-1252	293	21	c	c	NOUN
eurjchem-1252	293	22	for	for	ADP
eurjchem-1252	293	23	24‐48	24‐48	NUM
eurjchem-1252	293	24	h	h	NOUN
eurjchem-1252	293	25	,	,	PUNCT
eurjchem-1252	293	26	and	and	CCONJ
eurjchem-1252	293	27	yeast	yeast	NOUN
eurjchem-1252	293	28	at	at	ADP
eurjchem-1252	293	29	30	30	NUM
eurjchem-1252	293	30	°	°	NUM
eurjchem-1252	293	31	c	c	NOUN
eurjchem-1252	293	32	for	for	ADP
eurjchem-1252	293	33	24‐48	24‐48	NUM
eurjchem-1252	293	34	h.	h.	NOUN
eurjchem-1252	293	35	the	the	DET
eurjchem-1252	293	36	diameters	diameter	NOUN
eurjchem-1252	293	37	of	of	ADP
eurjchem-1252	293	38	the	the	DET
eurjchem-1252	293	39	inhibition	inhibition	NOUN
eurjchem-1252	293	40	zones	zone	NOUN
eurjchem-1252	293	41	(	(	PUNCT
eurjchem-1252	293	42	the	the	DET
eurjchem-1252	293	43	area	area	NOUN
eurjchem-1252	293	44	of	of	ADP
eurjchem-1252	293	45	no	no	DET
eurjchem-1252	293	46	growth	growth	NOUN
eurjchem-1252	293	47	of	of	ADP
eurjchem-1252	293	48	the	the	DET
eurjchem-1252	293	49	organism	organism	NOUN
eurjchem-1252	293	50	around	around	ADP
eurjchem-1252	293	51	the	the	DET
eurjchem-1252	293	52	disk	disk	NOUN
eurjchem-1252	293	53	)	)	PUNCT
eurjchem-1252	293	54	were	be	AUX
eurjchem-1252	293	55	measured	measure	VERB
eurjchem-1252	293	56	in	in	ADP
eurjchem-1252	293	57	millimetersusing	millimetersuse	VERB
eurjchem-1252	293	58	slipping	slip	VERB
eurjchem-1252	293	59	calipers	caliper	NOUN
eurjchem-1252	293	60	of	of	ADP
eurjchem-1252	293	61	national	national	PROPN
eurjchem-1252	293	62	committee	committee	PROPN
eurjchem-1252	293	63	for	for	ADP
eurjchem-1252	293	64	clinical	clinical	ADJ
eurjchem-1252	293	65	laboratory	laboratory	NOUN
eurjchem-1252	293	66	standards	standard	NOUN
eurjchem-1252	294	1	[	[	X
eurjchem-1252	294	2	9	9	NUM
eurjchem-1252	294	3	]	]	PUNCT
eurjchem-1252	294	4	.	.	PUNCT
eurjchem-1252	295	1	deeb	deeb	PROPN
eurjchem-1252	295	2	et	et	PROPN
eurjchem-1252	295	3	al	al	PROPN
eurjchem-1252	295	4	.	.	PUNCT
eurjchem-1252	295	5	/	/	SYM
eurjchem-1252	295	6	european	european	PROPN
eurjchem-1252	295	7	journal	journal	PROPN
eurjchem-1252	295	8	of	of	ADP
eurjchem-1252	295	9	chemistry	chemistry	NOUN
eurjchem-1252	295	10	6	6	NUM
eurjchem-1252	295	11	(	(	PUNCT
eurjchem-1252	295	12	2	2	NUM
eurjchem-1252	295	13	)	)	PUNCT
eurjchem-1252	295	14	(	(	PUNCT
eurjchem-1252	295	15	2015	2015	NUM
eurjchem-1252	295	16	)	)	PUNCT
eurjchem-1252	295	17	204‐210	204‐210	NOUN
eurjchem-1252	295	18	209	209	NUM
eurjchem-1252	295	19	table	table	NOUN
eurjchem-1252	295	20	1	1	NUM
eurjchem-1252	295	21	.	.	PUNCT
eurjchem-1252	295	22	antimicrobial	antimicrobial	ADJ
eurjchem-1252	295	23	activity	activity	NOUN
eurjchem-1252	295	24	of	of	ADP
eurjchem-1252	295	25	the	the	DET
eurjchem-1252	295	26	investigated	investigate	VERB
eurjchem-1252	295	27	conmpounds	conmpound	NOUN
eurjchem-1252	295	28	*	*	PUNCT
eurjchem-1252	295	29	.	.	PUNCT
eurjchem-1252	296	1	inhibition	inhibition	NOUN
eurjchem-1252	296	2	zone	zone	NOUN
eurjchem-1252	296	3	diameter	diameter	NOUN
eurjchem-1252	296	4	(	(	PUNCT
eurjchem-1252	296	5	mm	mm	PROPN
eurjchem-1252	296	6	/	/	SYM
eurjchem-1252	296	7	mg	mg	PROPN
eurjchem-1252	296	8	)	)	PUNCT
eurjchem-1252	296	9	sample	sample	NOUN
eurjchem-1252	296	10	compound	compound	NOUN
eurjchem-1252	296	11	aspergillus	aspergillus	PROPN
eurjchem-1252	296	12	flavuscandida	flavuscandida	PROPN
eurjchem-1252	296	13	albicans	albican	NOUN
eurjchem-1252	296	14	escherichia	escherichia	NOUN
eurjchem-1252	296	15	coli	coli	NOUN
eurjchem-1252	296	16	(	(	PUNCT
eurjchem-1252	296	17	g‐)staphylococcus	g‐)staphylococcus	PROPN
eurjchem-1252	296	18	aureus	aureus	PROPN
eurjchem-1252	296	19	(	(	PUNCT
eurjchem-1252	296	20	g+	g+	NOUN
eurjchem-1252	296	21	)	)	PUNCT
eurjchem-1252	296	22	‐	‐	ADV
eurjchem-1252	296	23	‐	‐	ADV
eurjchem-1252	296	24	+	+	NOUN
eurjchem-1252	297	1	+	+	X
eurjchem-1252	297	2	+	+	ADJ
eurjchem-1252	297	3	+	+	ADJ
eurjchem-1252	297	4	2	2	NUM
eurjchem-1252	297	5	‐	‐	NOUN
eurjchem-1252	297	6	‐	‐	ADV
eurjchem-1252	297	7	+	+	NOUN
eurjchem-1252	297	8	+	+	X
eurjchem-1252	297	9	+	+	ADJ
eurjchem-1252	297	10	+	+	X
eurjchem-1252	297	11	3b	3b	NOUN
eurjchem-1252	297	12	‐	‐	NOUN
eurjchem-1252	297	13	‐++++	‐++++	PUNCT
eurjchem-1252	297	14	3c	3c	NUM
eurjchem-1252	297	15	‐	‐	ADV
eurjchem-1252	297	16	‐++++	‐++++	PUNCT
eurjchem-1252	297	17	3d	3d	NOUN
eurjchem-1252	298	1	+	+	PUNCT
eurjchem-1252	298	2	+	+	ADJ
eurjchem-1252	298	3	+	+	ADJ
eurjchem-1252	298	4	+	+	ADJ
eurjchem-1252	298	5	+	+	ADJ
eurjchem-1252	298	6	+	+	ADJ
eurjchem-1252	298	7	+	+	ADJ
eurjchem-1252	298	8	4	4	NUM
eurjchem-1252	298	9	‐	‐	NOUN
eurjchem-1252	298	10	‐++++	‐++++	PUNCT
eurjchem-1252	298	11	5	5	NUM
eurjchem-1252	298	12	‐	‐	NOUN
eurjchem-1252	298	13	‐++++	‐++++	NUM
eurjchem-1252	298	14	6	6	NUM
eurjchem-1252	298	15	‐	‐	NOUN
eurjchem-1252	298	16	‐++++	‐++++	PUNCT
eurjchem-1252	298	17	7	7	NUM
eurjchem-1252	298	18	‐	‐	NOUN
eurjchem-1252	298	19	+	+	NOUN
eurjchem-1252	298	20	+	+	X
eurjchem-1252	298	21	+	+	ADJ
eurjchem-1252	298	22	+	+	ADJ
eurjchem-1252	298	23	+	+	ADJ
eurjchem-1252	298	24	+	+	ADJ
eurjchem-1252	298	25	+	+	NOUN
eurjchem-1252	298	26	8	8	NUM
eurjchem-1252	298	27	‐	‐	NOUN
eurjchem-1252	298	28	+	+	X
eurjchem-1252	299	1	+	+	PUNCT
eurjchem-1252	299	2	+	+	ADJ
eurjchem-1252	299	3	+	+	ADJ
eurjchem-1252	299	4	+	+	NUM
eurjchem-1252	299	5	10	10	NUM
eurjchem-1252	299	6	‐	‐	NOUN
eurjchem-1252	299	7	‐	‐	ADV
eurjchem-1252	299	8	+	+	NOUN
eurjchem-1252	299	9	+	+	X
eurjchem-1252	299	10	+	+	ADJ
eurjchem-1252	299	11	+	+	NOUN
eurjchem-1252	299	12	13	13	NUM
eurjchem-1252	299	13	‐	‐	NOUN
eurjchem-1252	299	14	‐++++	‐++++	NUM
eurjchem-1252	299	15	15	15	NUM
eurjchem-1252	299	16	‐	‐	NOUN
eurjchem-1252	299	17	‐	‐	ADV
eurjchem-1252	299	18	+	+	NOUN
eurjchem-1252	299	19	+	+	X
eurjchem-1252	299	20	+	+	ADJ
eurjchem-1252	299	21	+	+	NOUN
eurjchem-1252	299	22	16	16	NUM
eurjchem-1252	299	23	‐	‐	NOUN
eurjchem-1252	299	24	‐++++	‐++++	PUNCT
eurjchem-1252	299	25	17	17	NUM
eurjchem-1252	299	26	‐	‐	NOUN
eurjchem-1252	299	27	‐	‐	ADV
eurjchem-1252	299	28	‐	‐	ADP
eurjchem-1252	299	29	‐	‐	ADJ
eurjchem-1252	299	30	control	control	NOUN
eurjchem-1252	299	31	:	:	PUNCT
eurjchem-1252	299	32	dmso	dmso	NOUN
eurjchem-1252	299	33	‐	‐	VERB
eurjchem-1252	299	34	‐	‐	ADV
eurjchem-1252	299	35	+	+	NOUN
eurjchem-1252	300	1	+	+	X
eurjchem-1252	300	2	+	+	ADJ
eurjchem-1252	300	3	+	+	ADJ
eurjchem-1252	300	4	+	+	ADJ
eurjchem-1252	300	5	ampicillin	ampicillin	ADJ
eurjchem-1252	300	6	(	(	PUNCT
eurjchem-1252	300	7	antibacterial	antibacterial	ADJ
eurjchem-1252	300	8	agent	agent	NOUN
eurjchem-1252	300	9	)	)	PUNCT
eurjchem-1252	301	1	+	+	PUNCT
eurjchem-1252	301	2	+	+	X
eurjchem-1252	301	3	+	+	ADJ
eurjchem-1252	301	4	+	+	X
eurjchem-1252	301	5	‐	‐	NOUN
eurjchem-1252	301	6	‐	‐	ADV
eurjchem-1252	301	7	amphotericin	amphotericin	ADP
eurjchem-1252	301	8	b	b	NOUN
eurjchem-1252	301	9	(	(	PUNCT
eurjchem-1252	301	10	antifungal	antifungal	ADJ
eurjchem-1252	301	11	agent	agent	NOUN
eurjchem-1252	301	12	)	)	PUNCT
eurjchem-1252	302	1	*	*	PUNCT
eurjchem-1252	302	2	zone	zone	NOUN
eurjchem-1252	302	3	of	of	ADP
eurjchem-1252	302	4	inhibition	inhibition	NOUN
eurjchem-1252	302	5	:	:	PUNCT
eurjchem-1252	303	1	+	+	CCONJ
eurjchem-1252	303	2	=	=	SYM
eurjchem-1252	303	3	<	<	X
eurjchem-1252	303	4	11	11	NUM
eurjchem-1252	303	5	mm	mm	NOUN
eurjchem-1252	303	6	;	;	PUNCT
eurjchem-1252	303	7	+	+	X
eurjchem-1252	303	8	+	+	NUM
eurjchem-1252	303	9	=	=	SYM
eurjchem-1252	303	10	11‐20	11‐20	NUM
eurjchem-1252	303	11	mm	mm	NOUN
eurjchem-1252	303	12	;	;	PUNCT
eurjchem-1252	303	13	+	+	PROPN
eurjchem-1252	303	14	+	+	ADJ
eurjchem-1252	303	15	+	+	ADJ
eurjchem-1252	303	16	=	=	SYM
eurjchem-1252	303	17	20‐30	20‐30	NUM
eurjchem-1252	303	18	mm	mm	NOUN
eurjchem-1252	303	19	;	;	PUNCT
eurjchem-1252	303	20	‐	‐	NOUN
eurjchem-1252	303	21	=	=	NOUN
eurjchem-1252	303	22	no	no	DET
eurjchem-1252	303	23	inhibition	inhibition	NOUN
eurjchem-1252	303	24	.	.	PUNCT
eurjchem-1252	304	1	standard	standard	ADJ
eurjchem-1252	304	2	discs	disc	NOUN
eurjchem-1252	304	3	of	of	ADP
eurjchem-1252	304	4	ampicillin	ampicillin	NOUN
eurjchem-1252	304	5	(	(	PUNCT
eurjchem-1252	304	6	antibacterial	antibacterial	ADJ
eurjchem-1252	304	7	agent	agent	NOUN
eurjchem-1252	304	8	)	)	PUNCT
eurjchem-1252	304	9	,	,	PUNCT
eurjchem-1252	304	10	amphotericin	amphotericin	ADP
eurjchem-1252	304	11	b	b	X
eurjchem-1252	304	12	(	(	PUNCT
eurjchem-1252	304	13	antifungal	antifungal	ADJ
eurjchem-1252	304	14	agent	agent	NOUN
eurjchem-1252	304	15	)	)	PUNCT
eurjchem-1252	304	16	severed	sever	VERB
eurjchem-1252	304	17	as	as	ADP
eurjchem-1252	304	18	positive	positive	ADJ
eurjchem-1252	304	19	controls	control	NOUN
eurjchem-1252	304	20	for	for	ADP
eurjchem-1252	304	21	antimicrobial	antimicrobial	ADJ
eurjchem-1252	304	22	activity	activity	NOUN
eurjchem-1252	304	23	,	,	PUNCT
eurjchem-1252	304	24	but	but	CCONJ
eurjchem-1252	304	25	filter	filter	NOUN
eurjchem-1252	304	26	discs	disc	NOUN
eurjchem-1252	304	27	impregnated	impregnate	VERB
eurjchem-1252	304	28	with	with	ADP
eurjchem-1252	304	29	10	10	NUM
eurjchem-1252	304	30	μl	μl	ADP
eurjchem-1252	304	31	of	of	ADP
eurjchem-1252	304	32	dimethylsulfoxide	dimethylsulfoxide	ADJ
eurjchem-1252	304	33	were	be	AUX
eurjchem-1252	304	34	used	use	VERB
eurjchem-1252	304	35	as	as	ADP
eurjchem-1252	304	36	a	a	DET
eurjchem-1252	304	37	negative	negative	ADJ
eurjchem-1252	304	38	control	control	NOUN
eurjchem-1252	304	39	.	.	PUNCT
eurjchem-1252	305	1	blank	blank	ADJ
eurjchem-1252	305	2	paper	paper	NOUN
eurjchem-1252	305	3	discs	disc	NOUN
eurjchem-1252	305	4	(	(	PUNCT
eurjchem-1252	305	5	schleicher	schleicher	ADJ
eurjchem-1252	305	6	&	&	CCONJ
eurjchem-1252	305	7	schuell	schuell	PROPN
eurjchem-1252	305	8	,	,	PUNCT
eurjchem-1252	305	9	spain	spain	PROPN
eurjchem-1252	305	10	)	)	PUNCT
eurjchem-1252	305	11	with	with	ADP
eurjchem-1252	305	12	a	a	DET
eurjchem-1252	305	13	diameter	diameter	NOUN
eurjchem-1252	305	14	of	of	ADP
eurjchem-1252	305	15	8.0	8.0	NUM
eurjchem-1252	305	16	mm	mm	NOUN
eurjchem-1252	305	17	were	be	AUX
eurjchem-1252	305	18	impregnated	impregnate	VERB
eurjchem-1252	305	19	with	with	ADP
eurjchem-1252	305	20	10	10	NUM
eurjchem-1252	305	21	μl	μl	ADP
eurjchem-1252	305	22	of	of	ADP
eurjchem-1252	305	23	tested	test	VERB
eurjchem-1252	305	24	concentration	concentration	NOUN
eurjchem-1252	305	25	of	of	ADP
eurjchem-1252	305	26	the	the	DET
eurjchem-1252	305	27	stock	stock	NOUN
eurjchem-1252	305	28	solution	solution	NOUN
eurjchem-1252	305	29	.	.	PUNCT
eurjchem-1252	306	1	3	3	X
eurjchem-1252	306	2	.	.	NOUN
eurjchem-1252	306	3	results	result	NOUN
eurjchem-1252	306	4	and	and	CCONJ
eurjchem-1252	306	5	discussion	discussion	NOUN
eurjchem-1252	306	6	3.1	3.1	NUM
eurjchem-1252	306	7	.	.	PUNCT
eurjchem-1252	307	1	synthesis	synthesis	NOUN
eurjchem-1252	307	2	it	it	PRON
eurjchem-1252	307	3	was	be	AUX
eurjchem-1252	307	4	reported	report	VERB
eurjchem-1252	307	5	that	that	SCONJ
eurjchem-1252	307	6	the	the	DET
eurjchem-1252	307	7	reaction	reaction	NOUN
eurjchem-1252	307	8	of	of	ADP
eurjchem-1252	307	9	3‐amino‐4,5,6‐	3‐amino‐4,5,6‐	NUM
eurjchem-1252	307	10	triphenylpyridazine	triphenylpyridazine	NOUN
eurjchem-1252	307	11	with	with	ADP
eurjchem-1252	307	12	malonic	malonic	ADJ
eurjchem-1252	307	13	acid	acid	NOUN
eurjchem-1252	307	14	in	in	ADP
eurjchem-1252	307	15	presence	presence	NOUN
eurjchem-1252	307	16	of	of	ADP
eurjchem-1252	307	17	phosphoryl	phosphoryl	PROPN
eurjchem-1252	307	18	chloride	chloride	PROPN
eurjchem-1252	307	19	led	lead	VERB
eurjchem-1252	307	20	to	to	ADP
eurjchem-1252	307	21	the	the	DET
eurjchem-1252	307	22	pyrimido[1,2‐b]pyridazinone	pyrimido[1,2‐b]pyridazinone	NOUN
eurjchem-1252	307	23	derivative	derivative	NOUN
eurjchem-1252	307	24	,	,	PUNCT
eurjchem-1252	307	25	1	1	NUM
eurjchem-1252	307	26	[	[	X
eurjchem-1252	307	27	5	5	NUM
eurjchem-1252	307	28	]	]	PUNCT
eurjchem-1252	307	29	.	.	PUNCT
eurjchem-1252	308	1	the	the	DET
eurjchem-1252	308	2	various	various	ADJ
eurjchem-1252	308	3	reactions	reaction	NOUN
eurjchem-1252	308	4	of	of	ADP
eurjchem-1252	308	5	the	the	DET
eurjchem-1252	308	6	pyrimido	pyrimido	NOUN
eurjchem-1252	308	7	pyridazinone	pyridazinone	VERB
eurjchem-1252	308	8	derivative	derivative	ADJ
eurjchem-1252	308	9	1	1	NUM
eurjchem-1252	308	10	are	be	AUX
eurjchem-1252	308	11	shown	show	VERB
eurjchem-1252	308	12	in	in	ADP
eurjchem-1252	308	13	scheme	scheme	NOUN
eurjchem-1252	308	14	1	1	NUM
eurjchem-1252	308	15	.	.	PUNCT
eurjchem-1252	308	16	chlorination	chlorination	NOUN
eurjchem-1252	308	17	of	of	ADP
eurjchem-1252	308	18	compound	compound	NOUN
eurjchem-1252	308	19	1	1	NUM
eurjchem-1252	308	20	with	with	ADP
eurjchem-1252	308	21	phosphoryl	phosphoryl	PROPN
eurjchem-1252	308	22	chloride	chloride	PROPN
eurjchem-1252	308	23	led	lead	VERB
eurjchem-1252	308	24	to	to	ADP
eurjchem-1252	308	25	the	the	DET
eurjchem-1252	308	26	corresponding	correspond	VERB
eurjchem-1252	308	27	2‐chloro	2‐chloro	NUM
eurjchem-1252	308	28	derivative	derivative	ADJ
eurjchem-1252	308	29	,	,	PUNCT
eurjchem-1252	308	30	2	2	NUM
eurjchem-1252	308	31	.	.	PUNCT
eurjchem-1252	308	32	taking	take	VERB
eurjchem-1252	308	33	the	the	DET
eurjchem-1252	308	34	advantage	advantage	NOUN
eurjchem-1252	308	35	of	of	ADP
eurjchem-1252	308	36	the	the	DET
eurjchem-1252	308	37	reactivity	reactivity	NOUN
eurjchem-1252	308	38	of	of	ADP
eurjchem-1252	308	39	the	the	DET
eurjchem-1252	308	40	2‐chloro	2‐chloro	NUM
eurjchem-1252	308	41	atom	atom	NOUN
eurjchem-1252	308	42	in	in	ADP
eurjchem-1252	308	43	compound	compound	NOUN
eurjchem-1252	308	44	2	2	NUM
eurjchem-1252	308	45	,	,	PUNCT
eurjchem-1252	308	46	it	it	PRON
eurjchem-1252	308	47	was	be	AUX
eurjchem-1252	308	48	subjected	subject	VERB
eurjchem-1252	308	49	to	to	ADP
eurjchem-1252	308	50	nucleophilic	nucleophilic	ADJ
eurjchem-1252	308	51	substitution	substitution	NOUN
eurjchem-1252	308	52	reactions	reaction	NOUN
eurjchem-1252	308	53	in	in	ADP
eurjchem-1252	308	54	order	order	NOUN
eurjchem-1252	308	55	to	to	PART
eurjchem-1252	308	56	prepare	prepare	VERB
eurjchem-1252	308	57	other	other	ADJ
eurjchem-1252	308	58	derivatives	derivative	NOUN
eurjchem-1252	308	59	of	of	ADP
eurjchem-1252	308	60	the	the	DET
eurjchem-1252	308	61	system	system	NOUN
eurjchem-1252	308	62	.	.	PUNCT
eurjchem-1252	309	1	thus	thus	ADV
eurjchem-1252	309	2	,	,	PUNCT
eurjchem-1252	309	3	reaction	reaction	NOUN
eurjchem-1252	309	4	of	of	ADP
eurjchem-1252	309	5	compound	compound	NOUN
eurjchem-1252	309	6	2	2	NUM
eurjchem-1252	309	7	with	with	ADP
eurjchem-1252	309	8	sodium	sodium	NOUN
eurjchem-1252	309	9	methanolate	methanolate	ADJ
eurjchem-1252	309	10	,	,	PUNCT
eurjchem-1252	309	11	ethanolate	ethanolate	ADJ
eurjchem-1252	309	12	,	,	PUNCT
eurjchem-1252	309	13	sodium	sodium	NOUN
eurjchem-1252	309	14	azide	azide	NOUN
eurjchem-1252	309	15	,	,	PUNCT
eurjchem-1252	309	16	and	and	CCONJ
eurjchem-1252	309	17	hydrazine	hydrazine	NOUN
eurjchem-1252	309	18	hydrate	hydrate	NOUN
eurjchem-1252	309	19	,	,	PUNCT
eurjchem-1252	309	20	gave	give	VERB
eurjchem-1252	309	21	compounds	compound	NOUN
eurjchem-1252	309	22	3a‐d	3a‐d	ADV
eurjchem-1252	309	23	,	,	PUNCT
eurjchem-1252	309	24	respectively	respectively	ADV
eurjchem-1252	309	25	(	(	PUNCT
eurjchem-1252	309	26	scheme	scheme	NOUN
eurjchem-1252	309	27	1	1	NUM
eurjchem-1252	309	28	)	)	PUNCT
eurjchem-1252	309	29	.	.	PUNCT
eurjchem-1252	310	1	also	also	ADV
eurjchem-1252	310	2	,	,	PUNCT
eurjchem-1252	310	3	the	the	DET
eurjchem-1252	310	4	chloro	chloro	NOUN
eurjchem-1252	310	5	derivative	derivative	ADJ
eurjchem-1252	310	6	2	2	NUM
eurjchem-1252	310	7	underwent	underwent	NOUN
eurjchem-1252	310	8	thionation	thionation	NOUN
eurjchem-1252	310	9	with	with	ADP
eurjchem-1252	310	10	thiourea	thiourea	NOUN
eurjchem-1252	310	11	in	in	ADP
eurjchem-1252	310	12	refluxing	refluxing	NOUN
eurjchem-1252	310	13	ethanol	ethanol	NOUN
eurjchem-1252	310	14	leading	lead	VERB
eurjchem-1252	310	15	to	to	ADP
eurjchem-1252	310	16	thiouronium	thiouronium	NOUN
eurjchem-1252	310	17	salt	salt	NOUN
eurjchem-1252	310	18	,	,	PUNCT
eurjchem-1252	310	19	which	which	PRON
eurjchem-1252	310	20	can	can	AUX
eurjchem-1252	310	21	be	be	AUX
eurjchem-1252	310	22	isolated	isolate	VERB
eurjchem-1252	310	23	.	.	PUNCT
eurjchem-1252	311	1	the	the	DET
eurjchem-1252	311	2	7,8,9‐	7,8,9‐	NUM
eurjchem-1252	311	3	triphenyl‐2‐thioxo‐2h‐pyrimido[1,2‐b]pyridazin‐4(3h)‐one	triphenyl‐2‐thioxo‐2h‐pyrimido[1,2‐b]pyridazin‐4(3h)‐one	NUM
eurjchem-1252	311	4	(	(	PUNCT
eurjchem-1252	311	5	4	4	NUM
eurjchem-1252	311	6	)	)	PUNCT
eurjchem-1252	311	7	was	be	AUX
eurjchem-1252	311	8	obtained	obtain	VERB
eurjchem-1252	311	9	from	from	ADP
eurjchem-1252	311	10	the	the	DET
eurjchem-1252	311	11	thiouronium	thiouronium	NOUN
eurjchem-1252	311	12	salt	salt	NOUN
eurjchem-1252	311	13	in	in	ADP
eurjchem-1252	311	14	aqueous	aqueous	ADJ
eurjchem-1252	311	15	solution	solution	NOUN
eurjchem-1252	311	16	by	by	ADP
eurjchem-1252	311	17	basic	basic	ADJ
eurjchem-1252	311	18	hydrolysis	hydrolysis	NOUN
eurjchem-1252	311	19	followed	follow	VERB
eurjchem-1252	311	20	by	by	ADP
eurjchem-1252	311	21	acidification	acidification	NOUN
eurjchem-1252	311	22	with	with	ADP
eurjchem-1252	311	23	hydrochloric	hydrochloric	ADJ
eurjchem-1252	311	24	acid	acid	NOUN
eurjchem-1252	311	25	(	(	PUNCT
eurjchem-1252	311	26	scheme	scheme	NOUN
eurjchem-1252	311	27	1	1	NUM
eurjchem-1252	311	28	)	)	PUNCT
eurjchem-1252	311	29	.	.	PUNCT
eurjchem-1252	312	1	some	some	DET
eurjchem-1252	312	2	other	other	ADJ
eurjchem-1252	312	3	reactions	reaction	NOUN
eurjchem-1252	312	4	of	of	ADP
eurjchem-1252	312	5	compound	compound	NOUN
eurjchem-1252	312	6	1	1	NUM
eurjchem-1252	312	7	are	be	AUX
eurjchem-1252	312	8	shown	show	VERB
eurjchem-1252	312	9	in	in	ADP
eurjchem-1252	312	10	(	(	PUNCT
eurjchem-1252	312	11	scheme	scheme	NOUN
eurjchem-1252	312	12	2	2	NUM
eurjchem-1252	312	13	)	)	PUNCT
eurjchem-1252	312	14	.	.	PUNCT
eurjchem-1252	313	1	bromination	bromination	NOUN
eurjchem-1252	313	2	with	with	ADP
eurjchem-1252	313	3	an	an	DET
eurjchem-1252	313	4	excess	excess	NOUN
eurjchem-1252	313	5	of	of	ADP
eurjchem-1252	313	6	bromine	bromine	NOUN
eurjchem-1252	313	7	,	,	PUNCT
eurjchem-1252	313	8	a	a	DET
eurjchem-1252	313	9	dibromo	dibromo	NOUN
eurjchem-1252	313	10	derivative	derivative	ADJ
eurjchem-1252	313	11	5	5	NUM
eurjchem-1252	313	12	was	be	AUX
eurjchem-1252	313	13	obtained	obtain	VERB
eurjchem-1252	313	14	.	.	PUNCT
eurjchem-1252	314	1	chlorination	chlorination	NOUN
eurjchem-1252	314	2	of	of	ADP
eurjchem-1252	314	3	compound	compound	NOUN
eurjchem-1252	314	4	1	1	NUM
eurjchem-1252	314	5	with	with	ADP
eurjchem-1252	314	6	sulfuryl	sulfuryl	PROPN
eurjchem-1252	314	7	chloride	chloride	PROPN
eurjchem-1252	314	8	led	lead	VERB
eurjchem-1252	314	9	to	to	ADP
eurjchem-1252	314	10	3,3‐dichloro‐7,8,9‐triphenyl‐2h‐	3,3‐dichloro‐7,8,9‐triphenyl‐2h‐	NUM
eurjchem-1252	314	11	pyrimido[1,2‐b]pyridazine‐2,4(3h)‐dione,6	pyrimido[1,2‐b]pyridazine‐2,4(3h)‐dione,6	NOUN
eurjchem-1252	314	12	.	.	PUNCT
eurjchem-1252	315	1	the	the	DET
eurjchem-1252	315	2	usefulness	usefulness	NOUN
eurjchem-1252	315	3	of	of	ADP
eurjchem-1252	315	4	the	the	DET
eurjchem-1252	315	5	latter	latter	ADJ
eurjchem-1252	315	6	compound	compound	NOUN
eurjchem-1252	315	7	is	be	AUX
eurjchem-1252	315	8	demonstrated	demonstrate	VERB
eurjchem-1252	315	9	in	in	ADP
eurjchem-1252	315	10	(	(	PUNCT
eurjchem-1252	315	11	scheme	scheme	NOUN
eurjchem-1252	315	12	2	2	NUM
eurjchem-1252	315	13	)	)	PUNCT
eurjchem-1252	315	14	.	.	PUNCT
eurjchem-1252	316	1	the	the	DET
eurjchem-1252	316	2	ring	ring	NOUN
eurjchem-1252	316	3	contraction	contraction	NOUN
eurjchem-1252	316	4	of	of	ADP
eurjchem-1252	316	5	compound	compound	NOUN
eurjchem-1252	316	6	6	6	NUM
eurjchem-1252	316	7	was	be	AUX
eurjchem-1252	316	8	obtained	obtain	VERB
eurjchem-1252	316	9	on	on	ADP
eurjchem-1252	316	10	boiling	boil	VERB
eurjchem-1252	316	11	with	with	ADP
eurjchem-1252	316	12	aqueous	aqueous	ADJ
eurjchem-1252	316	13	solution	solution	NOUN
eurjchem-1252	316	14	of	of	ADP
eurjchem-1252	316	15	sodium	sodium	NOUN
eurjchem-1252	316	16	carbonate	carbonate	NOUN
eurjchem-1252	316	17	to	to	PART
eurjchem-1252	316	18	afford	afford	VERB
eurjchem-1252	316	19	3‐chloro	3‐chloro	NUM
eurjchem-1252	316	20	imidazo[1,2‐b]pyridazin‐2(3h)‐one	imidazo[1,2‐b]pyridazin‐2(3h)‐one	NOUN
eurjchem-1252	316	21	,	,	PUNCT
eurjchem-1252	316	22	7	7	NUM
eurjchem-1252	316	23	.	.	PUNCT
eurjchem-1252	317	1	however	however	ADV
eurjchem-1252	317	2	,	,	PUNCT
eurjchem-1252	317	3	reaction	reaction	NOUN
eurjchem-1252	317	4	of	of	ADP
eurjchem-1252	317	5	the	the	DET
eurjchem-1252	317	6	compound	compound	NOUN
eurjchem-1252	317	7	6	6	NUM
eurjchem-1252	317	8	with	with	ADP
eurjchem-1252	317	9	zinc	zinc	NOUN
eurjchem-1252	317	10	in	in	ADP
eurjchem-1252	317	11	acetic	acetic	ADJ
eurjchem-1252	317	12	acid	acid	NOUN
eurjchem-1252	317	13	at	at	ADP
eurjchem-1252	317	14	refluxing	refluxing	NOUN
eurjchem-1252	317	15	temperature	temperature	NOUN
eurjchem-1252	317	16	led	lead	VERB
eurjchem-1252	317	17	to	to	ADP
eurjchem-1252	317	18	3‐chloro	3‐chloro	NUM
eurjchem-1252	317	19	derivative	derivative	ADJ
eurjchem-1252	317	20	8	8	NUM
eurjchem-1252	317	21	in	in	ADP
eurjchem-1252	317	22	a	a	DET
eurjchem-1252	317	23	good	good	ADJ
eurjchem-1252	317	24	yield	yield	NOUN
eurjchem-1252	317	25	,	,	PUNCT
eurjchem-1252	317	26	which	which	PRON
eurjchem-1252	317	27	underwent	undergo	VERB
eurjchem-1252	317	28	direct	direct	ADJ
eurjchem-1252	317	29	amination	amination	NOUN
eurjchem-1252	317	30	by	by	ADP
eurjchem-1252	317	31	fusion	fusion	NOUN
eurjchem-1252	317	32	with	with	ADP
eurjchem-1252	317	33	ammonium	ammonium	NOUN
eurjchem-1252	317	34	acetate	acetate	NOUN
eurjchem-1252	317	35	at	at	ADP
eurjchem-1252	317	36	210	210	NUM
eurjchem-1252	317	37	°	°	ADP
eurjchem-1252	317	38	c	c	NOUN
eurjchem-1252	317	39	for	for	ADP
eurjchem-1252	317	40	30	30	NUM
eurjchem-1252	317	41	min	min	NOUN
eurjchem-1252	317	42	to	to	PART
eurjchem-1252	317	43	give	give	VERB
eurjchem-1252	317	44	3‐amino‐7,8,9‐triphenyl‐2h‐	3‐amino‐7,8,9‐triphenyl‐2h‐	NUM
eurjchem-1252	317	45	pyrimido[1,2‐b]pyridazine‐2,4(3h)‐dione	pyrimido[1,2‐b]pyridazine‐2,4(3h)‐dione	NOUN
eurjchem-1252	317	46	derivative	derivative	ADJ
eurjchem-1252	317	47	9	9	NUM
eurjchem-1252	317	48	.	.	PUNCT
eurjchem-1252	318	1	the	the	DET
eurjchem-1252	318	2	action	action	NOUN
eurjchem-1252	318	3	of	of	ADP
eurjchem-1252	318	4	nitric	nitric	ADJ
eurjchem-1252	318	5	acid	acid	NOUN
eurjchem-1252	318	6	in	in	ADP
eurjchem-1252	318	7	acetic	acetic	ADJ
eurjchem-1252	318	8	acid	acid	NOUN
eurjchem-1252	318	9	could	could	AUX
eurjchem-1252	318	10	be	be	AUX
eurjchem-1252	318	11	performed	perform	VERB
eurjchem-1252	318	12	using	use	VERB
eurjchem-1252	318	13	sodium	sodium	NOUN
eurjchem-1252	318	14	nitrite	nitrite	NOUN
eurjchem-1252	318	15	as	as	SCONJ
eurjchem-1252	318	16	catalyst	catalyst	NOUN
eurjchem-1252	318	17	led	lead	VERB
eurjchem-1252	318	18	to	to	ADP
eurjchem-1252	318	19	3‐nitropyrimidopyridazinone	3‐nitropyrimidopyridazinone	NUM
eurjchem-1252	318	20	derivative10	derivative10	NOUN
eurjchem-1252	318	21	.	.	PUNCT
eurjchem-1252	319	1	the	the	DET
eurjchem-1252	319	2	catalytic	catalytic	ADJ
eurjchem-1252	319	3	effect	effect	NOUN
eurjchem-1252	319	4	of	of	ADP
eurjchem-1252	319	5	sodium	sodium	NOUN
eurjchem-1252	319	6	nitrite	nitrite	NOUN
eurjchem-1252	319	7	can	can	AUX
eurjchem-1252	319	8	be	be	AUX
eurjchem-1252	319	9	explained	explain	VERB
eurjchem-1252	319	10	by	by	ADP
eurjchem-1252	319	11	an	an	DET
eurjchem-1252	319	12	initial	initial	ADJ
eurjchem-1252	319	13	nitrosation	nitrosation	NOUN
eurjchem-1252	319	14	of	of	ADP
eurjchem-1252	319	15	compound	compound	NOUN
eurjchem-1252	319	16	1	1	NUM
eurjchem-1252	319	17	in	in	ADP
eurjchem-1252	319	18	position	position	NOUN
eurjchem-1252	319	19	3	3	NUM
eurjchem-1252	319	20	and	and	CCONJ
eurjchem-1252	319	21	subsequent	subsequent	ADJ
eurjchem-1252	319	22	oxidation	oxidation	NOUN
eurjchem-1252	319	23	of	of	ADP
eurjchem-1252	319	24	the	the	DET
eurjchem-1252	319	25	nitroso	nitroso	NOUN
eurjchem-1252	319	26	group	group	NOUN
eurjchem-1252	319	27	to	to	ADP
eurjchem-1252	319	28	the	the	DET
eurjchem-1252	319	29	desired	desire	VERB
eurjchem-1252	319	30	nitro	nitro	NOUN
eurjchem-1252	319	31	group	group	NOUN
eurjchem-1252	320	1	[	[	X
eurjchem-1252	320	2	10].treatment	10].treatment	NUM
eurjchem-1252	320	3	of	of	ADP
eurjchem-1252	320	4	the	the	DET
eurjchem-1252	320	5	nitro	nitro	NOUN
eurjchem-1252	320	6	derivative	derivative	NOUN
eurjchem-1252	320	7	10	10	NUM
eurjchem-1252	320	8	with	with	ADP
eurjchem-1252	320	9	phosphoryl	phosphoryl	PROPN
eurjchem-1252	320	10	chloride	chloride	PROPN
eurjchem-1252	320	11	gave	give	VERB
eurjchem-1252	320	12	the	the	DET
eurjchem-1252	320	13	corresponding	correspond	VERB
eurjchem-1252	320	14	2‐chloro	2‐chloro	NUM
eurjchem-1252	320	15	deriva‐	deriva‐	ADV
eurjchem-1252	320	16	tive	tive	PROPN
eurjchem-1252	320	17	11	11	NUM
eurjchem-1252	320	18	.	.	PUNCT
eurjchem-1252	321	1	also	also	ADV
eurjchem-1252	321	2	,	,	PUNCT
eurjchem-1252	321	3	reduction	reduction	NOUN
eurjchem-1252	321	4	of	of	ADP
eurjchem-1252	321	5	compound	compound	NOUN
eurjchem-1252	321	6	10	10	NUM
eurjchem-1252	321	7	was	be	AUX
eurjchem-1252	321	8	carried	carry	VERB
eurjchem-1252	321	9	out	out	ADP
eurjchem-1252	321	10	with	with	ADP
eurjchem-1252	321	11	zinc	zinc	NOUN
eurjchem-1252	321	12	dust	dust	NOUN
eurjchem-1252	321	13	in	in	ADP
eurjchem-1252	321	14	acetic	acetic	ADJ
eurjchem-1252	321	15	acid	acid	NOUN
eurjchem-1252	321	16	at	at	ADP
eurjchem-1252	321	17	refluxing	refluxing	NOUN
eurjchem-1252	321	18	temperature	temperature	NOUN
eurjchem-1252	321	19	,	,	PUNCT
eurjchem-1252	321	20	and	and	CCONJ
eurjchem-1252	321	21	gave	give	VERB
eurjchem-1252	321	22	the	the	DET
eurjchem-1252	321	23	3‐amino	3‐amino	NUM
eurjchem-1252	321	24	derivative	derivative	ADJ
eurjchem-1252	321	25	9	9	NUM
eurjchem-1252	321	26	(	(	PUNCT
eurjchem-1252	321	27	scheme	scheme	NOUN
eurjchem-1252	321	28	2	2	NUM
eurjchem-1252	321	29	)	)	PUNCT
eurjchem-1252	321	30	.	.	PUNCT
eurjchem-1252	322	1	introduction	introduction	NOUN
eurjchem-1252	322	2	of	of	ADP
eurjchem-1252	322	3	an	an	DET
eurjchem-1252	322	4	acetyl	acetyl	NOUN
eurjchem-1252	322	5	group	group	NOUN
eurjchem-1252	322	6	into	into	ADP
eurjchem-1252	322	7	the	the	DET
eurjchem-1252	322	8	3‐position	3‐position	NUM
eurjchem-1252	322	9	of	of	ADP
eurjchem-1252	322	10	the	the	DET
eurjchem-1252	322	11	pyrimidopyridazinone	pyrimidopyridazinone	NOUN
eurjchem-1252	322	12	derivative	derivative	NOUN
eurjchem-1252	322	13	1	1	NUM
eurjchem-1252	322	14	was	be	AUX
eurjchem-1252	322	15	obtained	obtain	VERB
eurjchem-1252	322	16	by	by	ADP
eurjchem-1252	322	17	direct	direct	ADJ
eurjchem-1252	322	18	c‐	c‐	NOUN
eurjchem-1252	322	19	acetylation	acetylation	NOUN
eurjchem-1252	322	20	with	with	ADP
eurjchem-1252	322	21	acetic	acetic	ADJ
eurjchem-1252	322	22	acid	acid	NOUN
eurjchem-1252	322	23	in	in	ADP
eurjchem-1252	322	24	polyphosphoric	polyphosphoric	ADJ
eurjchem-1252	322	25	acid	acid	NOUN
eurjchem-1252	322	26	according	accord	VERB
eurjchem-1252	322	27	to	to	ADP
eurjchem-1252	322	28	known	know	VERB
eurjchem-1252	322	29	method	method	NOUN
eurjchem-1252	322	30	[	[	X
eurjchem-1252	322	31	11	11	NUM
eurjchem-1252	322	32	]	]	PUNCT
eurjchem-1252	322	33	,	,	PUNCT
eurjchem-1252	322	34	gave	give	VERB
eurjchem-1252	322	35	3‐acetyl	3‐acetyl	NUM
eurjchem-1252	322	36	pyrimidopyridazinone	pyrimidopyridazinone	NOUN
eurjchem-1252	322	37	derivative	derivative	NOUN
eurjchem-1252	322	38	12	12	NUM
eurjchem-1252	322	39	in	in	ADP
eurjchem-1252	322	40	good	good	ADJ
eurjchem-1252	322	41	yield	yield	NOUN
eurjchem-1252	322	42	.	.	PUNCT
eurjchem-1252	323	1	the	the	DET
eurjchem-1252	323	2	α	α	PROPN
eurjchem-1252	323	3	,	,	PUNCT
eurjchem-1252	323	4	β‐unsaturated	β‐unsaturate	VERB
eurjchem-1252	323	5	ketone	ketone	NOUN
eurjchem-1252	323	6	13	13	NUM
eurjchem-1252	323	7	was	be	AUX
eurjchem-1252	323	8	synthesized	synthesize	VERB
eurjchem-1252	323	9	employing	employ	VERB
eurjchem-1252	323	10	claisen‐schmidt	claisen‐schmidt	ADJ
eurjchem-1252	323	11	reaction	reaction	NOUN
eurjchem-1252	323	12	by	by	ADP
eurjchem-1252	323	13	treating	treat	VERB
eurjchem-1252	323	14	the	the	DET
eurjchem-1252	323	15	3‐acetyl	3‐acetyl	NUM
eurjchem-1252	323	16	derivative	derivative	NOUN
eurjchem-1252	323	17	12	12	NUM
eurjchem-1252	323	18	with	with	ADP
eurjchem-1252	323	19	benzaldehyde	benzaldehyde	NOUN
eurjchem-1252	323	20	in	in	ADP
eurjchem-1252	323	21	presence	presence	NOUN
eurjchem-1252	323	22	of	of	ADP
eurjchem-1252	323	23	base	base	NOUN
eurjchem-1252	323	24	.	.	PUNCT
eurjchem-1252	324	1	refluxing	refluxing	NOUN
eurjchem-1252	324	2	compound	compound	NOUN
eurjchem-1252	324	3	12	12	NUM
eurjchem-1252	324	4	with	with	ADP
eurjchem-1252	324	5	phosphoryl	phosphoryl	PROPN
eurjchem-1252	324	6	chloride	chloride	PROPN
eurjchem-1252	324	7	gave	give	VERB
eurjchem-1252	324	8	the	the	DET
eurjchem-1252	324	9	corresponding	correspond	VERB
eurjchem-1252	324	10	3‐acetyl‐2‐chloropyrimido	3‐acetyl‐2‐chloropyrimido	NUM
eurjchem-1252	324	11	pyridazinone	pyridazinone	NOUN
eurjchem-1252	324	12	derivative	derivative	ADJ
eurjchem-1252	324	13	14	14	NUM
eurjchem-1252	324	14	(	(	PUNCT
eurjchem-1252	324	15	scheme	scheme	NOUN
eurjchem-1252	324	16	3	3	NUM
eurjchem-1252	324	17	)	)	PUNCT
eurjchem-1252	324	18	.	.	PUNCT
eurjchem-1252	325	1	when	when	SCONJ
eurjchem-1252	325	2	the	the	DET
eurjchem-1252	325	3	1,3‐dinucleophilic	1,3‐dinucleophilic	PROPN
eurjchem-1252	325	4	7,8,9‐triphenyl‐2h‐pyrimido	7,8,9‐triphenyl‐2h‐pyrimido	NUM
eurjchem-1252	325	5	[	[	X
eurjchem-1252	325	6	1,2‐b]pyridazine‐2,4(3h)‐dione	1,2‐b]pyridazine‐2,4(3h)‐dione	NUM
eurjchem-1252	325	7	(	(	PUNCT
eurjchem-1252	325	8	1	1	NUM
eurjchem-1252	325	9	)	)	PUNCT
eurjchem-1252	325	10	was	be	AUX
eurjchem-1252	325	11	condensed	condense	VERB
eurjchem-1252	325	12	with	with	ADP
eurjchem-1252	325	13	diethyl	diethyl	NOUN
eurjchem-1252	325	14	malonate	malonate	NOUN
eurjchem-1252	325	15	at	at	ADP
eurjchem-1252	325	16	refluxing	refluxing	NOUN
eurjchem-1252	325	17	temperature	temperature	NOUN
eurjchem-1252	325	18	,	,	PUNCT
eurjchem-1252	325	19	furnished	furnish	VERB
eurjchem-1252	325	20	pyrano	pyrano	NOUN
eurjchem-1252	325	21	pyrimidopyridazinone	pyrimidopyridazinone	NOUN
eurjchem-1252	325	22	derivative	derivative	ADJ
eurjchem-1252	325	23	15	15	NUM
eurjchem-1252	325	24	(	(	PUNCT
eurjchem-1252	325	25	scheme	scheme	NOUN
eurjchem-1252	325	26	3	3	NUM
eurjchem-1252	325	27	)	)	PUNCT
eurjchem-1252	325	28	.	.	PUNCT
eurjchem-1252	326	1	formylation	formylation	NOUN
eurjchem-1252	326	2	of	of	ADP
eurjchem-1252	326	3	compound	compound	NOUN
eurjchem-1252	326	4	1	1	NUM
eurjchem-1252	326	5	at	at	ADP
eurjchem-1252	326	6	position	position	NOUN
eurjchem-1252	326	7	3	3	NUM
eurjchem-1252	326	8	was	be	AUX
eurjchem-1252	326	9	achieved	achieve	VERB
eurjchem-1252	326	10	by	by	ADP
eurjchem-1252	326	11	its	its	PRON
eurjchem-1252	326	12	reaction	reaction	NOUN
eurjchem-1252	326	13	with	with	ADP
eurjchem-1252	326	14	chloroform	chloroform	NOUN
eurjchem-1252	326	15	/	/	SYM
eurjchem-1252	326	16	potassium	potassium	NOUN
eurjchem-1252	326	17	hydroxide	hydroxide	NOUN
eurjchem-1252	326	18	mixture	mixture	NOUN
eurjchem-1252	326	19	,	,	PUNCT
eurjchem-1252	326	20	and	and	CCONJ
eurjchem-1252	326	21	afforded	afford	VERB
eurjchem-1252	326	22	3‐	3‐	NUM
eurjchem-1252	326	23	(	(	PUNCT
eurjchem-1252	326	24	hydroxymethylidene)‐7	hydroxymethylidene)‐7	ADJ
eurjchem-1252	326	25	,	,	PUNCT
eurjchem-1252	326	26	8	8	NUM
eurjchem-1252	326	27	,	,	PUNCT
eurjchem-1252	326	28	9‐triphenyl‐2h‐pyrimido[1	9‐triphenyl‐2h‐pyrimido[1	PRON
eurjchem-1252	326	29	,	,	PUNCT
eurjchem-1252	326	30	2‐b	2‐b	NUM
eurjchem-1252	326	31	]	]	X
eurjchem-1252	326	32	pyridazine‐2,4(3h)‐dione	pyridazine‐2,4(3h)‐dione	NUM
eurjchem-1252	326	33	,	,	PUNCT
eurjchem-1252	326	34	16	16	NUM
eurjchem-1252	326	35	.	.	PUNCT
eurjchem-1252	327	1	however	however	ADV
eurjchem-1252	327	2	,	,	PUNCT
eurjchem-1252	327	3	reaction	reaction	NOUN
eurjchem-1252	327	4	of	of	ADP
eurjchem-1252	327	5	compound	compound	NOUN
eurjchem-1252	327	6	1	1	NUM
eurjchem-1252	327	7	with	with	ADP
eurjchem-1252	327	8	vilsmeier	vilsmeier	ADJ
eurjchem-1252	327	9	reagent	reagent	NOUN
eurjchem-1252	327	10	(	(	PUNCT
eurjchem-1252	327	11	dimethylformamide	dimethylformamide	NOUN
eurjchem-1252	327	12	/	/	SYM
eurjchem-1252	327	13	phosphoryl	phosphoryl	NOUN
eurjchem-1252	327	14	chloride	chloride	NOUN
eurjchem-1252	327	15	)	)	PUNCT
eurjchem-1252	327	16	led	lead	VERB
eurjchem-1252	327	17	to	to	ADP
eurjchem-1252	327	18	2‐chloro‐4‐oxo‐7,8,9‐triphenyl‐4h‐pyrimido	2‐chloro‐4‐oxo‐7,8,9‐triphenyl‐4h‐pyrimido	NUM
eurjchem-1252	327	19	[	[	X
eurjchem-1252	327	20	1,2‐b]pyridazine‐3‐carbaldehyde	1,2‐b]pyridazine‐3‐carbaldehyde	NUM
eurjchem-1252	327	21	17	17	NUM
eurjchem-1252	327	22	,	,	PUNCT
eurjchem-1252	327	23	which	which	PRON
eurjchem-1252	327	24	was	be	AUX
eurjchem-1252	327	25	also	also	ADV
eurjchem-1252	327	26	obtained	obtain	VERB
eurjchem-1252	327	27	by	by	ADP
eurjchem-1252	327	28	the	the	DET
eurjchem-1252	327	29	reaction	reaction	NOUN
eurjchem-1252	327	30	of	of	ADP
eurjchem-1252	327	31	compound	compound	NOUN
eurjchem-1252	327	32	16	16	NUM
eurjchem-1252	327	33	with	with	ADP
eurjchem-1252	327	34	phosphoryl	phosphoryl	PROPN
eurjchem-1252	327	35	chloride	chloride	PROPN
eurjchem-1252	327	36	at	at	ADP
eurjchem-1252	327	37	refluxing	refluxing	NOUN
eurjchem-1252	327	38	temperature	temperature	NOUN
eurjchem-1252	327	39	(	(	PUNCT
eurjchem-1252	327	40	scheme	scheme	NOUN
eurjchem-1252	327	41	3	3	NUM
eurjchem-1252	327	42	)	)	PUNCT
eurjchem-1252	327	43	.	.	PUNCT
eurjchem-1252	328	1	the	the	DET
eurjchem-1252	328	2	newly	newly	ADV
eurjchem-1252	328	3	synthesized	synthesize	VERB
eurjchem-1252	328	4	compounds	compound	NOUN
eurjchem-1252	328	5	were	be	AUX
eurjchem-1252	328	6	characterized	characterize	VERB
eurjchem-1252	328	7	by	by	ADP
eurjchem-1252	328	8	ir	ir	PROPN
eurjchem-1252	328	9	,	,	PUNCT
eurjchem-1252	328	10	nmr	nmr	NOUN
eurjchem-1252	328	11	and	and	CCONJ
eurjchem-1252	328	12	mass	mass	NOUN
eurjchem-1252	328	13	spect‐	spect‐	VERB
eurjchem-1252	328	14	rum	rum	NOUN
eurjchem-1252	328	15	as	as	ADV
eurjchem-1252	328	16	well	well	ADV
eurjchem-1252	328	17	as	as	ADP
eurjchem-1252	328	18	the	the	DET
eurjchem-1252	328	19	elemental	elemental	ADJ
eurjchem-1252	328	20	analysis	analysis	NOUN
eurjchem-1252	328	21	,	,	PUNCT
eurjchem-1252	328	22	listed	list	VERB
eurjchem-1252	328	23	in	in	ADP
eurjchem-1252	328	24	experimental	experimental	ADJ
eurjchem-1252	328	25	section	section	NOUN
eurjchem-1252	328	26	.	.	PUNCT
eurjchem-1252	329	1	the	the	DET
eurjchem-1252	329	2	spectral	spectral	ADJ
eurjchem-1252	329	3	analyses	analysis	NOUN
eurjchem-1252	329	4	were	be	AUX
eurjchem-1252	329	5	in	in	ADP
eurjchem-1252	329	6	accordance	accordance	NOUN
eurjchem-1252	329	7	with	with	ADP
eurjchem-1252	329	8	the	the	DET
eurjchem-1252	329	9	assigned	assign	VERB
eurjchem-1252	329	10	structures	structure	NOUN
eurjchem-1252	329	11	.	.	PUNCT
eurjchem-1252	330	1	3.2	3.2	NUM
eurjchem-1252	330	2	.	.	X
eurjchem-1252	331	1	screening	screen	VERB
eurjchem-1252	331	2	for	for	ADP
eurjchem-1252	331	3	antimicrobial	antimicrobial	ADJ
eurjchem-1252	331	4	activities	activity	NOUN
eurjchem-1252	331	5	the	the	DET
eurjchem-1252	331	6	given	give	VERB
eurjchem-1252	331	7	results	result	NOUN
eurjchem-1252	331	8	in	in	ADP
eurjchem-1252	331	9	table	table	NOUN
eurjchem-1252	331	10	1	1	NUM
eurjchem-1252	331	11	revealed	reveal	VERB
eurjchem-1252	331	12	that	that	SCONJ
eurjchem-1252	331	13	compound	compound	NOUN
eurjchem-1252	331	14	8	8	NUM
eurjchem-1252	331	15	was	be	AUX
eurjchem-1252	331	16	highly	highly	ADV
eurjchem-1252	331	17	active	active	ADJ
eurjchem-1252	331	18	against	against	ADP
eurjchem-1252	331	19	staphylococcus	staphylococcus	NOUN
eurjchem-1252	331	20	aureus	aureus	NOUN
eurjchem-1252	331	21	.	.	PUNCT
eurjchem-1252	332	1	on	on	ADP
eurjchem-1252	332	2	the	the	DET
eurjchem-1252	332	3	other	other	ADJ
eurjchem-1252	332	4	hand	hand	NOUN
eurjchem-1252	332	5	,	,	PUNCT
eurjchem-1252	332	6	compounds	compound	VERB
eurjchem-1252	332	7	2	2	NUM
eurjchem-1252	332	8	,	,	PUNCT
eurjchem-1252	332	9	3b‐d	3b‐d	NUM
eurjchem-1252	332	10	,	,	PUNCT
eurjchem-1252	332	11	4‐7	4‐7	NOUN
eurjchem-1252	332	12	,	,	PUNCT
eurjchem-1252	332	13	10	10	NUM
eurjchem-1252	332	14	,	,	PUNCT
eurjchem-1252	332	15	13	13	NUM
eurjchem-1252	332	16	,	,	PUNCT
eurjchem-1252	332	17	15	15	NUM
eurjchem-1252	332	18	,	,	PUNCT
eurjchem-1252	332	19	16	16	NUM
eurjchem-1252	332	20	and	and	CCONJ
eurjchem-1252	332	21	17	17	NUM
eurjchem-1252	332	22	)	)	PUNCT
eurjchem-1252	332	23	showed	show	VERB
eurjchem-1252	332	24	moderate	moderate	ADJ
eurjchem-1252	332	25	activity	activity	NOUN
eurjchem-1252	332	26	against	against	ADP
eurjchem-1252	332	27	both	both	DET
eurjchem-1252	332	28	staphylococcus	staphylococcus	NOUN
eurjchem-1252	332	29	aureus	aureus	NOUN
eurjchem-1252	332	30	and	and	CCONJ
eurjchem-1252	332	31	escherichia	escherichia	NOUN
eurjchem-1252	332	32	coli	coli	NOUN
eurjchem-1252	332	33	.	.	PUNCT
eurjchem-1252	333	1	also	also	ADV
eurjchem-1252	333	2	,	,	PUNCT
eurjchem-1252	333	3	the	the	DET
eurjchem-1252	333	4	results	result	NOUN
eurjchem-1252	333	5	indicated	indicate	VERB
eurjchem-1252	333	6	that	that	SCONJ
eurjchem-1252	333	7	compounds	compound	VERB
eurjchem-1252	333	8	4	4	NUM
eurjchem-1252	333	9	and	and	CCONJ
eurjchem-1252	333	10	8	8	NUM
eurjchem-1252	333	11	showed	show	VERB
eurjchem-1252	333	12	moderate	moderate	ADJ
eurjchem-1252	333	13	antifungal	antifungal	ADJ
eurjchem-1252	333	14	activity	activity	NOUN
eurjchem-1252	333	15	against	against	ADP
eurjchem-1252	333	16	candida	candida	NOUN
eurjchem-1252	333	17	albicans	albican	NOUN
eurjchem-1252	333	18	.	.	PUNCT
eurjchem-1252	334	1	in	in	ADP
eurjchem-1252	334	2	general	general	ADJ
eurjchem-1252	334	3	,	,	PUNCT
eurjchem-1252	334	4	the	the	DET
eurjchem-1252	334	5	synthesised	synthesise	VERB
eurjchem-1252	334	6	compounds	compound	NOUN
eurjchem-1252	334	7	showed	show	VERB
eurjchem-1252	334	8	moderate	moderate	ADJ
eurjchem-1252	334	9	antimicrobial	antimicrobial	ADJ
eurjchem-1252	334	10	activity	activity	NOUN
eurjchem-1252	334	11	against	against	ADP
eurjchem-1252	334	12	the	the	DET
eurjchem-1252	334	13	examined	examine	VERB
eurjchem-1252	334	14	bacteria	bacteria	NOUN
eurjchem-1252	334	15	comparable	comparable	ADJ
eurjchem-1252	334	16	with	with	ADP
eurjchem-1252	334	17	the	the	DET
eurjchem-1252	334	18	standard	standard	ADJ
eurjchem-1252	334	19	antibacterial	antibacterial	ADJ
eurjchem-1252	334	20	ampicillin	ampicillin	NOUN
eurjchem-1252	334	21	.	.	PUNCT
eurjchem-1252	335	1	4	4	X
eurjchem-1252	335	2	.	.	X
eurjchem-1252	335	3	conclusion	conclusion	NOUN
eurjchem-1252	335	4	a	a	DET
eurjchem-1252	335	5	new	new	ADJ
eurjchem-1252	335	6	series	series	NOUN
eurjchem-1252	335	7	of	of	ADP
eurjchem-1252	335	8	pyrimidopyridazine	pyrimidopyridazine	NOUN
eurjchem-1252	335	9	bearing	bear	VERB
eurjchem-1252	335	10	different	different	ADJ
eurjchem-1252	335	11	substiutents	substiutent	NOUN
eurjchem-1252	335	12	were	be	AUX
eurjchem-1252	335	13	synthesized	synthesize	VERB
eurjchem-1252	335	14	and	and	CCONJ
eurjchem-1252	335	15	biological	biological	ADJ
eurjchem-1252	335	16	evaluation	evaluation	NOUN
eurjchem-1252	335	17	compound	compound	NOUN
eurjchem-1252	335	18	8	8	NUM
eurjchem-1252	335	19	showed	show	VERB
eurjchem-1252	335	20	promising	promise	VERB
eurjchem-1252	335	21	antibacterial	antibacterial	ADJ
eurjchem-1252	335	22	activities	activity	NOUN
eurjchem-1252	335	23	,	,	PUNCT
eurjchem-1252	335	24	compared	compare	VERB
eurjchem-1252	335	25	with	with	ADP
eurjchem-1252	335	26	the	the	DET
eurjchem-1252	335	27	reference	reference	NOUN
eurjchem-1252	335	28	drugs	drug	NOUN
eurjchem-1252	335	29	.	.	PUNCT
eurjchem-1252	336	1	210	210	NUM
eurjchem-1252	336	2	deeb	deeb	PROPN
eurjchem-1252	336	3	et	et	PROPN
eurjchem-1252	336	4	al	al	PROPN
eurjchem-1252	336	5	.	.	PUNCT
eurjchem-1252	336	6	/	/	SYM
eurjchem-1252	336	7	european	european	PROPN
eurjchem-1252	336	8	journal	journal	PROPN
eurjchem-1252	336	9	of	of	ADP
eurjchem-1252	336	10	chemistry	chemistry	NOUN
eurjchem-1252	336	11	6	6	NUM
eurjchem-1252	336	12	(	(	PUNCT
eurjchem-1252	336	13	2	2	NUM
eurjchem-1252	336	14	)	)	PUNCT
eurjchem-1252	336	15	(	(	PUNCT
eurjchem-1252	336	16	2015	2015	NUM
eurjchem-1252	336	17	)	)	PUNCT
eurjchem-1252	337	1	204‐210	204‐210	PROPN
eurjchem-1252	337	2	acknowledgement	acknowledgement	NOUN
eurjchem-1252	337	3	the	the	DET
eurjchem-1252	337	4	author	author	NOUN
eurjchem-1252	337	5	acknowledges	acknowledge	VERB
eurjchem-1252	337	6	the	the	DET
eurjchem-1252	337	7	help	help	NOUN
eurjchem-1252	337	8	of	of	ADP
eurjchem-1252	337	9	prof	prof	PROPN
eurjchem-1252	337	10	.	.	PUNCT
eurjchem-1252	338	1	yehia	yehia	PROPN
eurjchem-1252	338	2	ahmed	ahmed	PROPN
eurjchem-1252	338	3	el‐zawahry	el‐zawahry	PROPN
eurjchem-1252	338	4	,	,	PUNCT
eurjchem-1252	338	5	department	department	NOUN
eurjchem-1252	338	6	of	of	ADP
eurjchem-1252	338	7	microbiology	microbiology	NOUN
eurjchem-1252	338	8	for	for	ADP
eurjchem-1252	338	9	carrying	carry	VERB
eurjchem-1252	338	10	out	out	ADP
eurjchem-1252	338	11	the	the	DET
eurjchem-1252	338	12	antimicrobial	antimicrobial	ADJ
eurjchem-1252	338	13	activity	activity	NOUN
eurjchem-1252	338	14	.	.	PUNCT
eurjchem-1252	339	1	references	reference	NOUN
eurjchem-1252	339	2	[	[	X
eurjchem-1252	339	3	1	1	NUM
eurjchem-1252	339	4	]	]	PUNCT
eurjchem-1252	339	5	.	.	PUNCT
eurjchem-1252	340	1	deeb	deeb	PROPN
eurjchem-1252	340	2	,	,	PUNCT
eurjchem-1252	340	3	a.	a.	PROPN
eurjchem-1252	340	4	;	;	PUNCT
eurjchem-1252	340	5	shaqra	shaqra	PROPN
eurjchem-1252	340	6	,	,	PUNCT
eurjchem-1252	340	7	s.	s.	PROPN
eurjchem-1252	340	8	;	;	PUNCT
eurjchem-1252	340	9	abo	abo	NOUN
eurjchem-1252	340	10	elfotoh	elfotoh	NOUN
eurjchem-1252	340	11	,	,	PUNCT
eurjchem-1252	340	12	t.	t.	PROPN
eurjchem-1252	340	13	;	;	PUNCT
eurjchem-1252	340	14	dief	dief	PROPN
eurjchem-1252	340	15	,	,	PUNCT
eurjchem-1252	340	16	s.	s.	PROPN
eurjchem-1252	340	17	eur	eur	PROPN
eurjchem-1252	340	18	.	.	PUNCT
eurjchem-1252	340	19	chem	chem	PROPN
eurjchem-1252	340	20	.	.	PUNCT
eurjchem-1252	341	1	bull	bull	NOUN
eurjchem-1252	341	2	.	.	PUNCT
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eurjchem-1252	342	2	,	,	PUNCT
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eurjchem-1252	342	4	)	)	PUNCT
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eurjchem-1252	343	3	]	]	PUNCT
eurjchem-1252	343	4	.	.	PUNCT
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eurjchem-1252	345	3	]	]	PUNCT
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eurjchem-1252	347	3	]	]	PUNCT
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eurjchem-1252	363	2	.	.	PUNCT
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eurjchem-1252	364	2	,	,	PUNCT
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