id	sid	tid	token	lemma	pos
eurjchem-1358	1	1	untitled	untitled	ADJ
eurjchem-1358	1	2	issn	issn	PROPN
eurjchem-1358	1	3	215	215	NUM
eurjchem-1358	1	4	develop	develop	VERB
eurjchem-1358	1	5	the	the	DET
eurjchem-1358	1	6	simu	simu	NOUN
eurjchem-1358	1	7	degrada	degrada	PROPN
eurjchem-1358	1	8	mohamed	mohamed	PROPN
eurjchem-1358	1	9	ehab	ehab	PROPN
eurjchem-1358	1	10	faro	faro	PROPN
eurjchem-1358	1	11	1	1	NUM
eurjchem-1358	1	12	medicinal	medicinal	ADJ
eurjchem-1358	1	13	chem	chem	NOUN
eurjchem-1358	1	14	2	2	NUM
eurjchem-1358	1	15	pharmaceutica	pharmaceutica	NOUN
eurjchem-1358	1	16	3	3	NUM
eurjchem-1358	1	17	central	central	ADJ
eurjchem-1358	1	18	admin	admin	NOUN
eurjchem-1358	1	19	*	*	PUNCT
eurjchem-1358	1	20	corresponding	correspond	VERB
eurjchem-1358	1	21	tel	tel	PROPN
eurjchem-1358	1	22	.	.	PUNCT
eurjchem-1358	1	23	:	:	PUNCT
eurjchem-1358	2	1	+2.012.243	+2.012.243	PROPN
eurjchem-1358	2	2	article	article	NOUN
eurjchem-1358	2	3	in	in	ADP
eurjchem-1358	2	4	doi	doi	PROPN
eurjchem-1358	2	5	:	:	PUNCT
eurjchem-1358	2	6	10.5155	10.5155	NUM
eurjchem-1358	2	7	/	/	SYM
eurjchem-1358	2	8	e	e	NOUN
eurjchem-1358	2	9	received	receive	VERB
eurjchem-1358	2	10	:	:	PUNCT
eurjchem-1358	2	11	06	06	NUM
eurjchem-1358	2	12	no	no	PRON
eurjchem-1358	2	13	received	receive	VERB
eurjchem-1358	2	14	in	in	ADP
eurjchem-1358	2	15	rev	rev	PROPN
eurjchem-1358	2	16	accepted	accept	VERB
eurjchem-1358	2	17	:	:	PUNCT
eurjchem-1358	2	18	29	29	NUM
eurjchem-1358	2	19	no	no	DET
eurjchem-1358	2	20	published	publish	VERB
eurjchem-1358	2	21	onlin	onlin	NOUN
eurjchem-1358	2	22	printed	print	VERB
eurjchem-1358	2	23	:	:	PUNCT
eurjchem-1358	2	24	31	31	NUM
eurjchem-1358	2	25	mar	mar	PROPN
eurjchem-1358	2	26	keywords	keyword	NOUN
eurjchem-1358	2	27	rp‐lc	rp‐lc	VERB
eurjchem-1358	2	28	otilonium	otilonium	NOUN
eurjchem-1358	2	29	brom	brom	NOUN
eurjchem-1358	2	30	p‐aminobenzoi	p‐aminobenzoi	VERB
eurjchem-1358	2	31	stability	stability	NOUN
eurjchem-1358	2	32	indicat	indicat	VERB
eurjchem-1358	2	33	pharmaceutical	pharmaceutical	ADJ
eurjchem-1358	2	34	simultaneous	simultaneous	ADJ
eurjchem-1358	2	35	d	d	NOUN
eurjchem-1358	2	36	1	1	NUM
eurjchem-1358	2	37	.	.	PUNCT
eurjchem-1358	2	38	introduct	introduct	NOUN
eurjchem-1358	2	39	otiloniu	otiloniu	NOUN
eurjchem-1358	2	40	(	(	PUNCT
eurjchem-1358	2	41	octyloxy)ben	octyloxy)ben	NOUN
eurjchem-1358	2	42	(	(	PUNCT
eurjchem-1358	2	43	figure	figure	NOUN
eurjchem-1358	2	44	1	1	NUM
eurjchem-1358	2	45	)	)	PUNCT
eurjchem-1358	2	46	.	.	PUNCT
eurjchem-1358	3	1	derivatives	derivative	NOUN
eurjchem-1358	3	2	w	w	VERB
eurjchem-1358	3	3	hypersensiti	hypersensiti	INTJ
eurjchem-1358	3	4	particular	particular	ADJ
eurjchem-1358	3	5	fo	fo	ADP
eurjchem-1358	3	6	[	[	X
eurjchem-1358	3	7	1	1	NUM
eurjchem-1358	3	8	]	]	PUNCT
eurjchem-1358	3	9	.	.	PUNCT
eurjchem-1358	4	1	irritable	irritable	ADJ
eurjchem-1358	4	2	the	the	DET
eurjchem-1358	4	3	wide	wide	ADJ
eurjchem-1358	4	4	ran	run	VERB
eurjchem-1358	4	5	the	the	DET
eurjchem-1358	4	6	numerou	numerou	NOUN
eurjchem-1358	4	7	the	the	DET
eurjchem-1358	4	8	main	main	ADJ
eurjchem-1358	4	9	re	re	ADJ
eurjchem-1358	4	10	etiologic	etiologic	NOUN
eurjchem-1358	4	11	the	the	DET
eurjchem-1358	4	12	muscle	muscle	NOUN
eurjchem-1358	4	13	of	of	ADP
eurjchem-1358	4	14	th	th	PRON
eurjchem-1358	4	15	having	have	VERB
eurjchem-1358	4	16	a	a	DET
eurjchem-1358	4	17	loca	loca	NOUN
eurjchem-1358	4	18	furthermore	furthermore	ADV
eurjchem-1358	4	19	rapidly	rapidly	ADV
eurjchem-1358	4	20	elimi	elimi	VERB
eurjchem-1358	4	21	to	to	PART
eurjchem-1358	4	22	be	be	AUX
eurjchem-1358	4	23	well	well	ADV
eurjchem-1358	4	24	t	t	NOUN
eurjchem-1358	4	25	effects	effect	NOUN
eurjchem-1358	4	26	that	that	PRON
eurjchem-1358	4	27	muscarinic	muscarinic	NOUN
eurjchem-1358	4	28	s	s	PROPN
eurjchem-1358	4	29	53‐2249	53‐2249	NUM
eurjchem-1358	4	30	(	(	PUNCT
eurjchem-1358	4	31	print	print	NOUN
eurjchem-1358	4	32	)	)	PUNCT
eurjchem-1358	4	33	pment	pment	NOUN
eurjchem-1358	4	34	and	and	CCONJ
eurjchem-1358	4	35	ultaneous	ultaneous	ADJ
eurjchem-1358	4	36	ation	ation	PROPN
eurjchem-1358	4	37	prod	prod	NOUN
eurjchem-1358	4	38	d	d	PROPN
eurjchem-1358	4	39	mahmoud	mahmoud	PROPN
eurjchem-1358	4	40	ouk	ouk	PROPN
eurjchem-1358	4	41	elkady	elkady	PROPN
eurjchem-1358	4	42	2	2	PROPN
eurjchem-1358	4	43	mistry	mistry	PROPN
eurjchem-1358	4	44	department	department	PROPN
eurjchem-1358	4	45	al	al	PROPN
eurjchem-1358	4	46	chemistry	chemistry	PROPN
eurjchem-1358	4	47	depar	depar	NOUN
eurjchem-1358	4	48	istration	istration	NOUN
eurjchem-1358	4	49	for	for	ADP
eurjchem-1358	4	50	pharm	pharm	NOUN
eurjchem-1358	4	51	g	g	PROPN
eurjchem-1358	4	52	author	author	NOUN
eurjchem-1358	4	53	at	at	ADP
eurjchem-1358	4	54	:	:	PUNCT
eurjchem-1358	4	55	centra	centra	PROPN
eurjchem-1358	4	56	314304	314304	NUM
eurjchem-1358	4	57	.	.	PUNCT
eurjchem-1358	5	1	fax	fax	NOUN
eurjchem-1358	5	2	:	:	PUNCT
eurjchem-1358	5	3	+2.012	+2.012	NOUN
eurjchem-1358	5	4	formation	formation	NOUN
eurjchem-1358	5	5	eurjchem.7.1.97‐10	eurjchem.7.1.97‐10	NOUN
eurjchem-1358	5	6	ovember	ovember	NOUN
eurjchem-1358	5	7	2015	2015	NUM
eurjchem-1358	5	8	vised	vise	VERB
eurjchem-1358	5	9	form	form	NOUN
eurjchem-1358	5	10	:	:	PUNCT
eurjchem-1358	5	11	28	28	NUM
eurjchem-1358	5	12	nov	nov	PROPN
eurjchem-1358	5	13	ovember	ovember	PROPN
eurjchem-1358	5	14	2015	2015	NUM
eurjchem-1358	5	15	ne	ne	PROPN
eurjchem-1358	5	16	:	:	PUNCT
eurjchem-1358	5	17	31	31	NUM
eurjchem-1358	5	18	march	march	PROPN
eurjchem-1358	5	19	2016	2016	NUM
eurjchem-1358	5	20	rch	rch	NOUN
eurjchem-1358	5	21	2016	2016	NUM
eurjchem-1358	5	22	s	s	NOUN
eurjchem-1358	5	23	mide	mide	NOUN
eurjchem-1358	5	24	ic	ic	PROPN
eurjchem-1358	5	25	acid	acid	PROPN
eurjchem-1358	5	26	ting	ting	PROPN
eurjchem-1358	5	27	assay	assay	PROPN
eurjchem-1358	5	28	l	l	PROPN
eurjchem-1358	5	29	preparation	preparation	NOUN
eurjchem-1358	5	30	determination	determination	NOUN
eurjchem-1358	5	31	tion	tion	PROPN
eurjchem-1358	5	32	m	m	PROPN
eurjchem-1358	5	33	bromide	bromide	NOUN
eurjchem-1358	5	34	is	be	AUX
eurjchem-1358	5	35	nzoyl]amino}be	nzoyl]amino}be	NOUN
eurjchem-1358	5	36	ob	ob	PROPN
eurjchem-1358	5	37	is	be	AUX
eurjchem-1358	5	38	a	a	DET
eurjchem-1358	5	39	memb	memb	NOUN
eurjchem-1358	5	40	widely	widely	ADV
eurjchem-1358	5	41	used	use	VERB
eurjchem-1358	5	42	for	for	ADP
eurjchem-1358	5	43	vity	vity	NOUN
eurjchem-1358	5	44	disorders	disorder	NOUN
eurjchem-1358	5	45	r	r	VERB
eurjchem-1358	5	46	the	the	DET
eurjchem-1358	5	47	treatment	treatment	NOUN
eurjchem-1358	5	48	e	e	PROPN
eurjchem-1358	5	49	bowel	bowel	NOUN
eurjchem-1358	5	50	syndro	syndro	PROPN
eurjchem-1358	5	51	nge	nge	PROPN
eurjchem-1358	5	52	of	of	ADP
eurjchem-1358	5	53	symptom	symptom	NOUN
eurjchem-1358	5	54	us	us	PROPN
eurjchem-1358	5	55	pathological	pathological	ADJ
eurjchem-1358	5	56	eason	eason	NOUN
eurjchem-1358	5	57	of	of	ADP
eurjchem-1358	5	58	the	the	DET
eurjchem-1358	5	59	l	l	NOUN
eurjchem-1358	5	60	erapy	erapy	NOUN
eurjchem-1358	6	1	[	[	X
eurjchem-1358	6	2	2,3	2,3	NUM
eurjchem-1358	6	3	]	]	PUNCT
eurjchem-1358	6	4	.	.	PUNCT
eurjchem-1358	7	1	ob	ob	X
eurjchem-1358	7	2	e	e	NOUN
eurjchem-1358	7	3	colon	colon	NOUN
eurjchem-1358	7	4	and	and	CCONJ
eurjchem-1358	7	5	rec	rec	PROPN
eurjchem-1358	7	6	al	al	PROPN
eurjchem-1358	7	7	action	action	NOUN
eurjchem-1358	7	8	with	with	ADP
eurjchem-1358	7	9	n	n	DET
eurjchem-1358	7	10	e	e	NOUN
eurjchem-1358	7	11	,	,	PUNCT
eurjchem-1358	7	12	ob	ob	PRON
eurjchem-1358	7	13	does	do	AUX
eurjchem-1358	7	14	not	not	PART
eurjchem-1358	7	15	c	c	AUX
eurjchem-1358	7	16	inated	inate	VERB
eurjchem-1358	7	17	from	from	ADP
eurjchem-1358	7	18	ma	ma	PROPN
eurjchem-1358	7	19	tolerated	tolerate	VERB
eurjchem-1358	7	20	,	,	PUNCT
eurjchem-1358	7	21	and	and	CCONJ
eurjchem-1358	7	22	are	be	AUX
eurjchem-1358	7	23	typical	typical	ADJ
eurjchem-1358	7	24	spasmolytic	spasmolytic	ADJ
eurjchem-1358	7	25	age	age	NOUN
eurjchem-1358	7	26	e	e	NOUN
eurjchem-1358	7	27	/	/	SYM
eurjchem-1358	7	28	issn	issn	VERB
eurjchem-1358	7	29	2153‐225	2153‐225	NUM
eurjchem-1358	7	30	ht	ht	NOUN
eurjchem-1358	7	31	europ	europ	PROPN
eurjchem-1358	7	32	d	d	X
eurjchem-1358	7	33	validati	validati	NOUN
eurjchem-1358	7	34	s	s	NOUN
eurjchem-1358	7	35	determi	determi	NOUN
eurjchem-1358	7	36	duct	duct	NOUN
eurjchem-1358	7	37	in	in	ADP
eurjchem-1358	7	38	bu	bu	PROPN
eurjchem-1358	7	39	el‐kerdawy	el‐kerdawy	PROPN
eurjchem-1358	7	40	2	2	NUM
eurjchem-1358	7	41	and	and	CCONJ
eurjchem-1358	7	42	ahmed	ahmed	PROPN
eurjchem-1358	7	43	t	t	PROPN
eurjchem-1358	7	44	,	,	PUNCT
eurjchem-1358	7	45	faculty	faculty	NOUN
eurjchem-1358	7	46	of	of	ADP
eurjchem-1358	7	47	pharm	pharm	PROPN
eurjchem-1358	7	48	rtment	rtment	PROPN
eurjchem-1358	7	49	,	,	PUNCT
eurjchem-1358	7	50	faculty	faculty	NOUN
eurjchem-1358	7	51	of	of	ADP
eurjchem-1358	7	52	p	p	PROPN
eurjchem-1358	7	53	maceutical	maceutical	ADJ
eurjchem-1358	7	54	affairs	affair	NOUN
eurjchem-1358	7	55	,	,	PUNCT
eurjchem-1358	7	56	m	m	PROPN
eurjchem-1358	7	57	al	al	PROPN
eurjchem-1358	7	58	administration	administration	NOUN
eurjchem-1358	7	59	fo	fo	ADP
eurjchem-1358	7	60	2.24314304	2.24314304	NUM
eurjchem-1358	7	61	.	.	PUNCT
eurjchem-1358	8	1	e‐mai	e‐mai	PROPN
eurjchem-1358	8	2	01.1358	01.1358	PROPN
eurjchem-1358	8	3	ember	ember	VERB
eurjchem-1358	8	4	2015	2015	NUM
eurjchem-1358	8	5	n	n	CCONJ
eurjchem-1358	8	6	,	,	PUNCT
eurjchem-1358	8	7	n‐diethyl‐	n‐diethyl‐	PROPN
eurjchem-1358	8	8	enzoyl)oxy]etha	enzoyl)oxy]etha	NUM
eurjchem-1358	8	9	ber	ber	NOUN
eurjchem-1358	8	10	of	of	ADP
eurjchem-1358	8	11	the	the	DET
eurjchem-1358	8	12	qua	qua	NOUN
eurjchem-1358	8	13	the	the	DET
eurjchem-1358	8	14	treatment	treatment	NOUN
eurjchem-1358	8	15	of	of	ADP
eurjchem-1358	8	16	the	the	DET
eurjchem-1358	8	17	intesti	intesti	PROPN
eurjchem-1358	8	18	t	t	PROPN
eurjchem-1358	8	19	of	of	ADP
eurjchem-1358	8	20	irritable	irritable	ADJ
eurjchem-1358	8	21	bo	bo	PROPN
eurjchem-1358	8	22	ome	ome	PROPN
eurjchem-1358	8	23	is	be	AUX
eurjchem-1358	8	24	a	a	DET
eurjchem-1358	8	25	compl	compl	NOUN
eurjchem-1358	8	26	ms	ms	NOUN
eurjchem-1358	8	27	can	can	AUX
eurjchem-1358	8	28	not	not	PART
eurjchem-1358	8	29	be	be	AUX
eurjchem-1358	8	30	a	a	DET
eurjchem-1358	8	31	mechanisms	mechanism	NOUN
eurjchem-1358	8	32	h	h	NOUN
eurjchem-1358	8	33	acking	acke	VERB
eurjchem-1358	8	34	of	of	ADP
eurjchem-1358	8	35	an	an	DET
eurjchem-1358	8	36	b	b	PROPN
eurjchem-1358	8	37	shows	show	VERB
eurjchem-1358	8	38	specifi	specifi	PROPN
eurjchem-1358	8	39	ctum	ctum	NOUN
eurjchem-1358	8	40	at	at	ADP
eurjchem-1358	8	41	therape	therape	NOUN
eurjchem-1358	8	42	negligible	negligible	ADJ
eurjchem-1358	8	43	system	system	NOUN
eurjchem-1358	8	44	cross	cross	VERB
eurjchem-1358	8	45	the	the	DET
eurjchem-1358	8	46	blood	blood	NOUN
eurjchem-1358	8	47	ajor	ajor	NOUN
eurjchem-1358	8	48	organs	organ	NOUN
eurjchem-1358	8	49	[	[	X
eurjchem-1358	8	50	7	7	NUM
eurjchem-1358	8	51	]	]	PUNCT
eurjchem-1358	8	52	.	.	PUNCT
eurjchem-1358	9	1	it	it	PRON
eurjchem-1358	9	2	seems	seem	VERB
eurjchem-1358	9	3	to	to	PART
eurjchem-1358	9	4	be	be	AUX
eurjchem-1358	9	5	of	of	ADP
eurjchem-1358	9	6	the	the	DET
eurjchem-1358	9	7	system	system	NOUN
eurjchem-1358	9	8	ents	ent	NOUN
eurjchem-1358	9	9	[	[	X
eurjchem-1358	9	10	5,8	5,8	NUM
eurjchem-1358	9	11	]	]	PUNCT
eurjchem-1358	9	12	.	.	PUNCT
eurjchem-1358	10	1	european	european	PROPN
eurjchem-1358	10	2	journa	journa	PROPN
eurjchem-1358	10	3	europ	europ	PROPN
eurjchem-1358	10	4	57	57	NUM
eurjchem-1358	10	5	(	(	PUNCT
eurjchem-1358	10	6	online	online	ADJ
eurjchem-1358	10	7	)	)	PUNCT
eurjchem-1358	10	8			NOUN
eurjchem-1358	11	1	20	20	NUM
eurjchem-1358	11	2	ttp://dx.doi.org/	ttp://dx.doi.org/	PROPN
eurjchem-1358	11	3	pean	pean	PROPN
eurjchem-1358	11	4	jo	jo	PROPN
eurjchem-1358	11	5	journal	journal	PROPN
eurjchem-1358	11	6	web	web	NOUN
eurjchem-1358	11	7	on	on	ADP
eurjchem-1358	11	8	of	of	ADP
eurjchem-1358	11	9	a	a	DET
eurjchem-1358	11	10	st	st	PROPN
eurjchem-1358	11	11	nation	nation	NOUN
eurjchem-1358	11	12	of	of	ADP
eurjchem-1358	11	13	ulk	ulk	PROPN
eurjchem-1358	11	14	drug	drug	PROPN
eurjchem-1358	11	15	a	a	DET
eurjchem-1358	11	16	y	y	PROPN
eurjchem-1358	11	17	1	1	NUM
eurjchem-1358	11	18	,	,	PUNCT
eurjchem-1358	11	19	ramzia	ramzia	PROPN
eurjchem-1358	12	1	i	i	PROPN
eurjchem-1358	12	2	d	d	PROPN
eurjchem-1358	12	3	adel	adel	PROPN
eurjchem-1358	12	4	othm	othm	PROPN
eurjchem-1358	12	5	acy	acy	PROPN
eurjchem-1358	12	6	,	,	PUNCT
eurjchem-1358	12	7	mansoura	mansoura	ADJ
eurjchem-1358	12	8	uni	uni	PROPN
eurjchem-1358	12	9	pharmacy	pharmacy	PROPN
eurjchem-1358	12	10	,	,	PUNCT
eurjchem-1358	12	11	cairo	cairo	PROPN
eurjchem-1358	12	12	un	un	PROPN
eurjchem-1358	12	13	manyal	manyal	PROPN
eurjchem-1358	12	14	,	,	PUNCT
eurjchem-1358	12	15	cairo	cairo	PROPN
eurjchem-1358	12	16	1156	1156	NUM
eurjchem-1358	12	17	or	or	CCONJ
eurjchem-1358	12	18	pharmaceutical	pharmaceutical	NOUN
eurjchem-1358	12	19	a	a	DET
eurjchem-1358	12	20	l	l	NOUN
eurjchem-1358	12	21	address	address	NOUN
eurjchem-1358	12	22	:	:	PUNCT
eurjchem-1358	13	1	a.osman8	a.osman8	NOUN
eurjchem-1358	13	2	abstract	abstract	ADJ
eurjchem-1358	13	3	a	a	DET
eurjchem-1358	13	4	simple	simple	NOUN
eurjchem-1358	13	5	,	,	PUNCT
eurjchem-1358	13	6	pre	pre	ADJ
eurjchem-1358	13	7	been	be	AUX
eurjchem-1358	13	8	develop	develop	VERB
eurjchem-1358	13	9	expected	expect	VERB
eurjchem-1358	13	10	de	de	X
eurjchem-1358	13	11	pharmaceutic	pharmaceutic	NOUN
eurjchem-1358	13	12	on	on	ADP
eurjchem-1358	13	13	waters	water	NOUN
eurjchem-1358	13	14	atl	atl	PROPN
eurjchem-1358	13	15	(	(	PUNCT
eurjchem-1358	13	16	ph	ph	PROPN
eurjchem-1358	13	17	=	=	SYM
eurjchem-1358	13	18	2.35	2.35	NUM
eurjchem-1358	13	19	)	)	PUNCT
eurjchem-1358	13	20	co	co	NOUN
eurjchem-1358	13	21	was	be	AUX
eurjchem-1358	13	22	0.8	0.8	NUM
eurjchem-1358	13	23	ml	ml	NOUN
eurjchem-1358	13	24	/	/	SYM
eurjchem-1358	13	25	m	m	NOUN
eurjchem-1358	13	26	range	range	NOUN
eurjchem-1358	13	27	of	of	ADP
eurjchem-1358	13	28	0.5‐1	0.5‐1	NOUN
eurjchem-1358	13	29	of	of	ADP
eurjchem-1358	13	30	1‐50	1‐50	NUM
eurjchem-1358	13	31	μg	μg	PROPN
eurjchem-1358	13	32	/	/	SYM
eurjchem-1358	13	33	m	m	PROPN
eurjchem-1358	13	34	were	be	AUX
eurjchem-1358	13	35	found	find	VERB
eurjchem-1358	13	36	to	to	ADP
eurjchem-1358	13	37	respectively	respectively	ADV
eurjchem-1358	13	38	.	.	PUNCT
eurjchem-1358	14	1	applied	apply	VERB
eurjchem-1358	14	2	to	to	ADP
eurjchem-1358	14	3	the	the	DET
eurjchem-1358	14	4	cite	cite	VERB
eurjchem-1358	14	5	this	this	PRON
eurjchem-1358	14	6	:	:	PUNCT
eurjchem-1358	14	7	eur	eur	ADJ
eurjchem-1358	14	8	.	.	PUNCT
eurjchem-1358	15	1	n‐methyl‐2‐[(4	n‐methyl‐2‐[(4	NOUN
eurjchem-1358	15	2	anaminium	anaminium	PROPN
eurjchem-1358	15	3	bro	bro	PROPN
eurjchem-1358	15	4	aternary	aternary	PROPN
eurjchem-1358	15	5	ammo	ammo	NOUN
eurjchem-1358	15	6	of	of	ADP
eurjchem-1358	15	7	hypermotilit	hypermotilit	PROPN
eurjchem-1358	15	8	ine	ine	PROPN
eurjchem-1358	15	9	,	,	PUNCT
eurjchem-1358	15	10	and	and	CCONJ
eurjchem-1358	15	11	is	be	AUX
eurjchem-1358	15	12	us	we	PRON
eurjchem-1358	15	13	owel	owel	PROPN
eurjchem-1358	15	14	syndrome	syndrome	PROPN
eurjchem-1358	15	15	ex	ex	PUNCT
eurjchem-1358	15	16	disease	disease	NOUN
eurjchem-1358	15	17	,	,	PUNCT
eurjchem-1358	15	18	in	in	ADP
eurjchem-1358	15	19	w	w	PROPN
eurjchem-1358	15	20	always	always	ADV
eurjchem-1358	15	21	attribut	attribut	PROPN
eurjchem-1358	15	22	hypothesized	hypothesize	VERB
eurjchem-1358	15	23	.	.	PUNCT
eurjchem-1358	16	1	t	t	PROPN
eurjchem-1358	16	2	appropriate	appropriate	NOUN
eurjchem-1358	16	3	sp	sp	ADP
eurjchem-1358	16	4	icity	icity	NOUN
eurjchem-1358	16	5	for	for	ADP
eurjchem-1358	16	6	the	the	DET
eurjchem-1358	16	7	sm	sm	PROPN
eurjchem-1358	16	8	eutic	eutic	PROPN
eurjchem-1358	16	9	concentra	concentra	PROPN
eurjchem-1358	16	10	mic	mic	ADJ
eurjchem-1358	16	11	absorption	absorption	NOUN
eurjchem-1358	16	12	d‐brain	d‐brain	NOUN
eurjchem-1358	16	13	barrier	barrier	NOUN
eurjchem-1358	16	14	.	.	PUNCT
eurjchem-1358	17	1	ob	ob	PROPN
eurjchem-1358	17	2	has	have	AUX
eurjchem-1358	17	3	been	be	AUX
eurjchem-1358	17	4	s	s	PROPN
eurjchem-1358	17	5	e	e	NOUN
eurjchem-1358	17	6	devoid	devoid	ADJ
eurjchem-1358	17	7	of	of	ADP
eurjchem-1358	17	8	the	the	DET
eurjchem-1358	17	9	mically	mically	ADV
eurjchem-1358	17	10	acting	act	VERB
eurjchem-1358	17	11	al	al	PROPN
eurjchem-1358	17	12	of	of	ADP
eurjchem-1358	17	13	chemistry	chemistry	PROPN
eurjchem-1358	17	14	7	7	NUM
eurjchem-1358	17	15	pean	pean	ADJ
eurjchem-1358	17	16	journal	journal	NOUN
eurjchem-1358	17	17	of	of	ADP
eurjchem-1358	17	18	c	c	PROPN
eurjchem-1358	17	19	016	016	NUM
eurjchem-1358	17	20	atlanta	atlanta	PROPN
eurjchem-1358	17	21	pub	pub	NOUN
eurjchem-1358	17	22	/10.5155	/10.5155	PROPN
eurjchem-1358	17	23	/	/	SYM
eurjchem-1358	17	24	eurjch	eurjch	PROPN
eurjchem-1358	17	25	ournal	ournal	ADJ
eurjchem-1358	17	26	bpage	bpage	NOUN
eurjchem-1358	17	27	:	:	PUNCT
eurjchem-1358	17	28	www	www	NOUN
eurjchem-1358	17	29	.	.	PUNCT
eurjchem-1358	18	1	tability‐in	tability‐in	PROPN
eurjchem-1358	18	2	f	f	PROPN
eurjchem-1358	18	3	otilonium	otilonium	NOUN
eurjchem-1358	18	4	and	and	CCONJ
eurjchem-1358	18	5	pharm	pharm	NOUN
eurjchem-1358	18	6	smail	smail	NOUN
eurjchem-1358	18	7	el‐bag	el‐bag	DET
eurjchem-1358	18	8	man	man	NOUN
eurjchem-1358	18	9	3	3	NUM
eurjchem-1358	18	10	,	,	PUNCT
eurjchem-1358	18	11	*	*	PUNCT
eurjchem-1358	18	12	iversity	iversity	NOUN
eurjchem-1358	18	13	,	,	PUNCT
eurjchem-1358	18	14	mansoura	mansoura	ADJ
eurjchem-1358	18	15	3	3	NUM
eurjchem-1358	18	16	niversity	niversity	NOUN
eurjchem-1358	18	17	,	,	PUNCT
eurjchem-1358	18	18	cairo	cairo	PROPN
eurjchem-1358	18	19	115	115	NUM
eurjchem-1358	18	20	62	62	NUM
eurjchem-1358	18	21	,	,	PUNCT
eurjchem-1358	18	22	egypt	egypt	PROPN
eurjchem-1358	18	23	affairs	affairs	PROPN
eurjchem-1358	18	24	,	,	PUNCT
eurjchem-1358	18	25	manyal	manyal	PROPN
eurjchem-1358	18	26	,	,	PUNCT
eurjchem-1358	18	27	ca	can	AUX
eurjchem-1358	18	28	88@yahoo.com	88@yahoo.com	NUM
eurjchem-1358	18	29	(	(	PUNCT
eurjchem-1358	18	30	a.	a.	NOUN
eurjchem-1358	18	31	cise	cise	PROPN
eurjchem-1358	18	32	,	,	PUNCT
eurjchem-1358	18	33	accurate	accurate	ADJ
eurjchem-1358	18	34	an	an	DET
eurjchem-1358	18	35	ped	ped	NOUN
eurjchem-1358	18	36	for	for	ADP
eurjchem-1358	18	37	the	the	DET
eurjchem-1358	18	38	sim	sim	ADJ
eurjchem-1358	18	39	gradation	gradation	NOUN
eurjchem-1358	18	40	prod	prod	NOUN
eurjchem-1358	18	41	cal	cal	PROPN
eurjchem-1358	18	42	preparation	preparation	NOUN
eurjchem-1358	18	43	.	.	PUNCT
eurjchem-1358	19	1	lantis	lantis	PROPN
eurjchem-1358	19	2	c18	c18	PROPN
eurjchem-1358	19	3	colum	colum	PROPN
eurjchem-1358	19	4	ontaining	ontaine	VERB
eurjchem-1358	19	5	0.05	0.05	NUM
eurjchem-1358	19	6	%	%	NOUN
eurjchem-1358	19	7	min	min	NOUN
eurjchem-1358	19	8	with	with	ADP
eurjchem-1358	19	9	uv	uv	PROPN
eurjchem-1358	19	10	det	det	PROPN
eurjchem-1358	19	11	100	100	NUM
eurjchem-1358	19	12	μg	μg	PROPN
eurjchem-1358	19	13	/	/	SYM
eurjchem-1358	19	14	ml	ml	NOUN
eurjchem-1358	19	15	with	with	ADP
eurjchem-1358	19	16	ml	ml	NOUN
eurjchem-1358	19	17	with	with	ADP
eurjchem-1358	19	18	regressi	regressi	PROPN
eurjchem-1358	19	19	o	o	PROPN
eurjchem-1358	19	20	be	be	AUX
eurjchem-1358	19	21	0.0665	0.0665	NUM
eurjchem-1358	19	22	and	and	CCONJ
eurjchem-1358	19	23	the	the	DET
eurjchem-1358	19	24	method	method	NOUN
eurjchem-1358	19	25	wa	wa	PROPN
eurjchem-1358	19	26	e	e	PROPN
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eurjchem-1358	19	28	.	.	PUNCT
eurjchem-1358	20	1	j.	j.	PROPN
eurjchem-1358	20	2	chem	chem	PROPN
eurjchem-1358	20	3	.	.	PUNCT
eurjchem-1358	21	1	2016	2016	NUM
eurjchem-1358	21	2	,	,	PUNCT
eurjchem-1358	21	3	4‐{[2‐	4‐{[2‐	NUM
eurjchem-1358	21	4	omide	omide	NOUN
eurjchem-1358	21	5	onium	onium	NOUN
eurjchem-1358	21	6	ty	ty	NOUN
eurjchem-1358	21	7	and	and	CCONJ
eurjchem-1358	21	8	sed	se	VERB
eurjchem-1358	21	9	in	in	ADP
eurjchem-1358	21	10	e	e	PROPN
eurjchem-1358	21	11	(	(	PUNCT
eurjchem-1358	21	12	ibs	ibs	PROPN
eurjchem-1358	21	13	)	)	PUNCT
eurjchem-1358	21	14	which	which	PRON
eurjchem-1358	21	15	ted	te	VERB
eurjchem-1358	21	16	to	to	ADP
eurjchem-1358	21	17	that	that	PRON
eurjchem-1358	21	18	is	be	AUX
eurjchem-1358	21	19	pecific	pecific	ADJ
eurjchem-1358	21	20	mooth	mooth	ADJ
eurjchem-1358	21	21	ations	ation	NOUN
eurjchem-1358	21	22	,	,	PUNCT
eurjchem-1358	22	1	[	[	X
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eurjchem-1358	22	3	]	]	PUNCT
eurjchem-1358	22	4	.	.	PUNCT
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eurjchem-1358	23	4	e	e	NOUN
eurjchem-1358	23	5	side	side	NOUN
eurjchem-1358	23	6	anti‐	anti‐	PROPN
eurjchem-1358	23	7	for	for	ADP
eurjchem-1358	23	8	biol	biol	NOUN
eurjchem-1358	23	9	[	[	X
eurjchem-1358	23	10	6,1	6,1	NUM
eurjchem-1358	23	11	mix	mix	NOUN
eurjchem-1358	23	12	[	[	PUNCT
eurjchem-1358	23	13	13	13	NUM
eurjchem-1358	23	14	figu	figu	VERB
eurjchem-1358	23	15	7	7	NUM
eurjchem-1358	23	16	(	(	PUNCT
eurjchem-1358	23	17	1	1	NUM
eurjchem-1358	23	18	)	)	PUNCT
eurjchem-1358	23	19	(	(	PUNCT
eurjchem-1358	23	20	2016	2016	NUM
eurjchem-1358	23	21	)	)	PUNCT
eurjchem-1358	23	22	97‐1	97‐1	NUM
eurjchem-1358	23	23	chemistry	chemistry	NOUN
eurjchem-1358	23	24	lishing	lishe	VERB
eurjchem-1358	23	25	house	house	NOUN
eurjchem-1358	23	26	ll	ll	AUX
eurjchem-1358	23	27	hem.7.1.97‐101.1	hem.7.1.97‐101.1	PROPN
eurjchem-1358	23	28	of	of	ADP
eurjchem-1358	23	29	che	che	PROPN
eurjchem-1358	24	1	.eurjchem.co	.eurjchem.co	X
eurjchem-1358	24	2	ndicating	ndicate	VERB
eurjchem-1358	24	3	r	r	NOUN
eurjchem-1358	24	4	m	m	PROPN
eurjchem-1358	24	5	bromid	bromid	PROPN
eurjchem-1358	24	6	maceutica	maceutica	PROPN
eurjchem-1358	24	7	gary	gary	PROPN
eurjchem-1358	24	8	2	2	NUM
eurjchem-1358	24	9	,	,	PUNCT
eurjchem-1358	24	10	35516	35516	NUM
eurjchem-1358	24	11	,	,	PUNCT
eurjchem-1358	24	12	egypt	egypt	PROPN
eurjchem-1358	24	13	562	562	NUM
eurjchem-1358	24	14	,	,	PUNCT
eurjchem-1358	24	15	egypt	egypt	PROPN
eurjchem-1358	24	16	airo	airo	PROPN
eurjchem-1358	24	17	11562	11562	NUM
eurjchem-1358	24	18	,	,	PUNCT
eurjchem-1358	24	19	egypt	egypt	PROPN
eurjchem-1358	24	20	.	.	PUNCT
eurjchem-1358	25	1	a.	a.	PROPN
eurjchem-1358	25	2	othman	othman	PROPN
eurjchem-1358	25	3	)	)	PUNCT
eurjchem-1358	25	4	.	.	PUNCT
eurjchem-1358	26	1	nd	nd	PRON
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eurjchem-1358	26	3	stabilit	stabilit	ADJ
eurjchem-1358	26	4	multaneous	multaneous	ADJ
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eurjchem-1358	26	6	duct	duct	NOUN
eurjchem-1358	26	7	;	;	PUNCT
eurjchem-1358	26	8	p‐aminob	p‐aminob	PUNCT
eurjchem-1358	26	9	chromatograph	chromatograph	PROPN
eurjchem-1358	26	10	mn	mn	PROPN
eurjchem-1358	26	11	(	(	PUNCT
eurjchem-1358	26	12	4.6	4.6	NUM
eurjchem-1358	26	13	×	×	NOUN
eurjchem-1358	26	14	150	150	NUM
eurjchem-1358	26	15	m	m	NOUN
eurjchem-1358	26	16	%	%	NOUN
eurjchem-1358	26	17	tfa	tfa	NOUN
eurjchem-1358	26	18	:	:	PUNCT
eurjchem-1358	26	19	acetonitri	acetonitri	VERB
eurjchem-1358	26	20	tection	tection	NOUN
eurjchem-1358	26	21	at	at	ADP
eurjchem-1358	26	22	290	290	NUM
eurjchem-1358	26	23	n	n	NOUN
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eurjchem-1358	26	25	coef	coef	PROPN
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eurjchem-1358	26	27	coefficient	coefficient	NOUN
eurjchem-1358	27	1	o	o	X
eurjchem-1358	27	2	d	d	X
eurjchem-1358	27	3	0.2018	0.2018	NUM
eurjchem-1358	27	4	μg	μg	PROPN
eurjchem-1358	27	5	/	/	SYM
eurjchem-1358	27	6	ml	ml	NOUN
eurjchem-1358	27	7	as	as	ADV
eurjchem-1358	27	8	validated	validate	VERB
eurjchem-1358	27	9	as	as	ADP
eurjchem-1358	27	10	p	p	NOUN
eurjchem-1358	27	11	of	of	ADP
eurjchem-1358	27	12	the	the	DET
eurjchem-1358	27	13	drug	drug	NOUN
eurjchem-1358	27	14	in	in	ADP
eurjchem-1358	27	15	bu	bu	PROPN
eurjchem-1358	27	16	7(1	7(1	PROPN
eurjchem-1358	27	17	)	)	PUNCT
eurjchem-1358	27	18	,	,	PUNCT
eurjchem-1358	27	19	97‐101	97‐101	PRON
eurjchem-1358	27	20	there	there	PRON
eurjchem-1358	27	21	are	be	VERB
eurjchem-1358	27	22	few	few	ADJ
eurjchem-1358	27	23	analysis	analysis	NOUN
eurjchem-1358	27	24	of	of	ADP
eurjchem-1358	27	25	oti	oti	PROPN
eurjchem-1358	27	26	logical	logical	ADJ
eurjchem-1358	27	27	fluids	fluid	NOUN
eurjchem-1358	27	28	in	in	ADP
eurjchem-1358	27	29	11	11	NUM
eurjchem-1358	27	30	]	]	PUNCT
eurjchem-1358	27	31	and	and	CCONJ
eurjchem-1358	27	32	lc‐ms/	lc‐ms/	PROPN
eurjchem-1358	27	33	xtures	xture	NOUN
eurjchem-1358	27	34	with	with	ADP
eurjchem-1358	27	35	be	be	AUX
eurjchem-1358	27	36	]	]	PUNCT
eurjchem-1358	27	37	and	and	CCONJ
eurjchem-1358	27	38	spectroph	spectroph	VERB
eurjchem-1358	27	39	ure	ure	PROPN
eurjchem-1358	27	40	1	1	NUM
eurjchem-1358	27	41	.	.	PUNCT
eurjchem-1358	28	1	chemical	chemical	NOUN
eurjchem-1358	28	2	str	str	VERB
eurjchem-1358	28	3	101	101	NUM
eurjchem-1358	28	4	lc	lc	NOUN
eurjchem-1358	28	5	‐	‐	ADP
eurjchem-1358	28	6	all	all	DET
eurjchem-1358	28	7	rights	right	NOUN
eurjchem-1358	28	8	re	re	ADP
eurjchem-1358	28	9	1358	1358	NUM
eurjchem-1358	28	10	emistry	emistry	NOUN
eurjchem-1358	28	11	m	m	NOUN
eurjchem-1358	28	12	rp‐lc	rp‐lc	NUM
eurjchem-1358	28	13	me	i	PRON
eurjchem-1358	28	14	de	de	ADP
eurjchem-1358	28	15	and	and	CCONJ
eurjchem-1358	28	16	its	its	PRON
eurjchem-1358	28	17	al	al	PROPN
eurjchem-1358	28	18	prepara	prepara	NOUN
eurjchem-1358	28	19	ty	ty	NUM
eurjchem-1358	28	20	indicating	indicate	VERB
eurjchem-1358	28	21	liqu	liqu	NOUN
eurjchem-1358	28	22	ermination	ermination	NOUN
eurjchem-1358	28	23	of	of	ADP
eurjchem-1358	28	24	o	o	NOUN
eurjchem-1358	28	25	benzoic	benzoic	NOUN
eurjchem-1358	28	26	acid	acid	NOUN
eurjchem-1358	28	27	(	(	PUNCT
eurjchem-1358	28	28	ic	ic	PROPN
eurjchem-1358	28	29	separation	separation	NOUN
eurjchem-1358	28	30	wa	wa	PROPN
eurjchem-1358	28	31	mm	mm	PROPN
eurjchem-1358	28	32	,	,	PUNCT
eurjchem-1358	28	33	5	5	NUM
eurjchem-1358	28	34	µm	µm	NOUN
eurjchem-1358	28	35	)	)	PUNCT
eurjchem-1358	28	36	using	use	VERB
eurjchem-1358	28	37	ile	ile	PROPN
eurjchem-1358	28	38	(	(	PUNCT
eurjchem-1358	28	39	30:70	30:70	NUM
eurjchem-1358	28	40	,	,	PUNCT
eurjchem-1358	28	41	v	v	NOUN
eurjchem-1358	28	42	:	:	SYM
eurjchem-1358	28	43	v	v	NOUN
eurjchem-1358	28	44	)	)	PUNCT
eurjchem-1358	28	45	a	a	DET
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eurjchem-1358	28	47	.	.	PUNCT
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eurjchem-1358	29	2	wa	wa	PROPN
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eurjchem-1358	29	5	1	1	NUM
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eurjchem-1358	29	7	o	o	NOUN
eurjchem-1358	29	8	of	of	ADP
eurjchem-1358	29	9	0.9998	0.9998	NUM
eurjchem-1358	29	10	for	for	ADP
eurjchem-1358	29	11	pa	pa	PROPN
eurjchem-1358	29	12	l	l	PROPN
eurjchem-1358	29	13	for	for	ADP
eurjchem-1358	29	14	ob	ob	NUM
eurjchem-1358	29	15	and	and	CCONJ
eurjchem-1358	29	16	0.1	0.1	NUM
eurjchem-1358	29	17	per	per	ADP
eurjchem-1358	29	18	ich	ich	PROPN
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eurjchem-1358	29	20	ulk	ulk	PROPN
eurjchem-1358	29	21	powder	powder	NOUN
eurjchem-1358	29	22	and	and	CCONJ
eurjchem-1358	29	23	w	w	NOUN
eurjchem-1358	29	24	analytical	analytical	ADJ
eurjchem-1358	29	25	me	i	PRON
eurjchem-1358	29	26	ilonium	ilonium	NOUN
eurjchem-1358	29	27	bromid	bromid	ADJ
eurjchem-1358	29	28	ncluding	nclude	VERB
eurjchem-1358	29	29	lc	lc	PROPN
eurjchem-1358	29	30	wit	wit	NOUN
eurjchem-1358	29	31	/ms	/ms	PUNCT
eurjchem-1358	30	1	[	[	X
eurjchem-1358	30	2	12	12	NUM
eurjchem-1358	30	3	]	]	PUNCT
eurjchem-1358	30	4	.	.	PUNCT
eurjchem-1358	31	1	besid	besid	PROPN
eurjchem-1358	31	2	enzodiazepines	enzodiazepines	PROPN
eurjchem-1358	31	3	hotometric	hotometric	ADV
eurjchem-1358	31	4	met	meet	VERB
eurjchem-1358	31	5	o	o	NOUN
eurjchem-1358	31	6	n	n	DET
eurjchem-1358	31	7	h	h	NOUN
eurjchem-1358	32	1	o	o	NOUN
eurjchem-1358	32	2	o	o	X
eurjchem-1358	32	3	h2n	h2n	PROPN
eurjchem-1358	32	4	ructures	ructure	NOUN
eurjchem-1358	32	5	of	of	ADP
eurjchem-1358	32	6	ob	ob	X
eurjchem-1358	32	7	(	(	PUNCT
eurjchem-1358	32	8	a	a	PRON
eurjchem-1358	32	9	)	)	PUNCT
eurjchem-1358	32	10	served	serve	VERB
eurjchem-1358	32	11	‐	‐	NOUN
eurjchem-1358	32	12	printed	print	VERB
eurjchem-1358	32	13	y	y	PROPN
eurjchem-1358	32	14	ethod	ethod	NOUN
eurjchem-1358	32	15	for	for	ADP
eurjchem-1358	32	16	expected	expect	VERB
eurjchem-1358	32	17	ation	ation	PROPN
eurjchem-1358	32	18	uid	uid	PROPN
eurjchem-1358	32	19	chromatogra	chromatogra	PROPN
eurjchem-1358	32	20	otilonium	otilonium	NOUN
eurjchem-1358	32	21	brom	brom	NOUN
eurjchem-1358	32	22	(	(	PUNCT
eurjchem-1358	32	23	paba	paba	PROPN
eurjchem-1358	32	24	)	)	PUNCT
eurjchem-1358	32	25	in	in	ADP
eurjchem-1358	32	26	bu	bu	ADV
eurjchem-1358	32	27	as	as	SCONJ
eurjchem-1358	32	28	carried	carry	VERB
eurjchem-1358	32	29	out	out	ADP
eurjchem-1358	32	30	by	by	ADP
eurjchem-1358	32	31	g	g	PROPN
eurjchem-1358	32	32	2	2	NUM
eurjchem-1358	32	33	mm	mm	NOUN
eurjchem-1358	32	34	ammoniu	ammoniu	NOUN
eurjchem-1358	32	35	as	as	ADP
eurjchem-1358	32	36	the	the	DET
eurjchem-1358	32	37	mobile	mobile	ADJ
eurjchem-1358	32	38	ph	ph	NOUN
eurjchem-1358	32	39	as	as	SCONJ
eurjchem-1358	32	40	obtained	obtain	VERB
eurjchem-1358	32	41	ove	ove	NOUN
eurjchem-1358	32	42	ob	ob	NOUN
eurjchem-1358	32	43	,	,	PUNCT
eurjchem-1358	32	44	and	and	CCONJ
eurjchem-1358	32	45	over	over	ADP
eurjchem-1358	32	46	con	con	X
eurjchem-1358	32	47	aba	aba	PROPN
eurjchem-1358	32	48	.	.	PUNCT
eurjchem-1358	33	1	the	the	DET
eurjchem-1358	33	2	values	value	NOUN
eurjchem-1358	33	3	1974	1974	NUM
eurjchem-1358	33	4	and	and	CCONJ
eurjchem-1358	33	5	0.598	0.598	NUM
eurjchem-1358	33	6	nes	ne	NOUN
eurjchem-1358	33	7	.	.	PUNCT
eurjchem-1358	34	1	the	the	DET
eurjchem-1358	34	2	method	method	ADJ
eurjchem-1358	34	3	pharmaceutical	pharmaceutical	NOUN
eurjchem-1358	34	4	ethods	ethod	NOUN
eurjchem-1358	34	5	reported	report	VERB
eurjchem-1358	34	6	de	de	ADP
eurjchem-1358	34	7	either	either	CCONJ
eurjchem-1358	34	8	in	in	ADP
eurjchem-1358	34	9	do	do	AUX
eurjchem-1358	34	10	th	th	X
eurjchem-1358	34	11	uv	uv	NOUN
eurjchem-1358	34	12	detection	detection	NOUN
eurjchem-1358	34	13	des	des	PROPN
eurjchem-1358	34	14	,	,	PUNCT
eurjchem-1358	34	15	it	it	PRON
eurjchem-1358	34	16	has	have	AUX
eurjchem-1358	34	17	been	be	AUX
eurjchem-1358	34	18	by	by	ADP
eurjchem-1358	34	19	capillary	capillary	ADJ
eurjchem-1358	34	20	e	e	NOUN
eurjchem-1358	34	21	thods	thod	NOUN
eurjchem-1358	34	22	[	[	X
eurjchem-1358	34	23	14‐17	14‐17	NUM
eurjchem-1358	34	24	]	]	X
eurjchem-1358	34	25	.	.	PUNCT
eurjchem-1358	35	1	o	o	X
eurjchem-1358	35	2	o	o	NOUN
eurjchem-1358	35	3	n+	n+	INTJ
eurjchem-1358	35	4	br	br	X
eurjchem-1358	35	5	(	(	PUNCT
eurjchem-1358	35	6	o	o	NOUN
eurjchem-1358	35	7	oh	oh	INTJ
eurjchem-1358	35	8	(	(	PUNCT
eurjchem-1358	35	9	b	b	NOUN
eurjchem-1358	35	10	)	)	PUNCT
eurjchem-1358	35	11	and	and	CCONJ
eurjchem-1358	35	12	its	its	PRON
eurjchem-1358	35	13	degraded	degraded	ADJ
eurjchem-1358	35	14	p	p	X
eurjchem-1358	35	15	d	d	PROPN
eurjchem-1358	35	16	in	in	ADP
eurjchem-1358	35	17	the	the	DET
eurjchem-1358	35	18	usa	usa	PROPN
eurjchem-1358	35	19	d	d	PROPN
eurjchem-1358	35	20	aphy	aphy	NOUN
eurjchem-1358	35	21	method	method	NOUN
eurjchem-1358	35	22	ha	ha	INTJ
eurjchem-1358	35	23	ide	ide	NOUN
eurjchem-1358	35	24	(	(	PUNCT
eurjchem-1358	35	25	ob	ob	NOUN
eurjchem-1358	35	26	)	)	PUNCT
eurjchem-1358	35	27	and	and	CCONJ
eurjchem-1358	35	28	i	i	PRON
eurjchem-1358	35	29	ulk	ulk	PROPN
eurjchem-1358	35	30	powder	powder	VERB
eurjchem-1358	35	31	an	an	DET
eurjchem-1358	35	32	y	y	PROPN
eurjchem-1358	35	33	isocratic	isocratic	PROPN
eurjchem-1358	35	34	elutio	elutio	NOUN
eurjchem-1358	35	35	um	um	INTJ
eurjchem-1358	35	36	acetate	acetate	PROPN
eurjchem-1358	35	37	buff	buff	PROPN
eurjchem-1358	35	38	ase	ase	PROPN
eurjchem-1358	35	39	.	.	PUNCT
eurjchem-1358	36	1	the	the	DET
eurjchem-1358	36	2	flow	flow	NOUN
eurjchem-1358	36	3	ra	ra	PROPN
eurjchem-1358	36	4	er	er	INTJ
eurjchem-1358	36	5	a	a	DET
eurjchem-1358	36	6	concentratio	concentratio	NOUN
eurjchem-1358	36	7	ncentration	ncentration	NOUN
eurjchem-1358	36	8	rang	ring	VERB
eurjchem-1358	36	9	of	of	ADP
eurjchem-1358	36	10	lod	lod	PROPN
eurjchem-1358	36	11	and	and	CCONJ
eurjchem-1358	36	12	lo	lo	PROPN
eurjchem-1358	36	13	μg	μg	PROPN
eurjchem-1358	36	14	/	/	SYM
eurjchem-1358	36	15	ml	ml	PROPN
eurjchem-1358	36	16	for	for	ADP
eurjchem-1358	36	17	pab	pab	NOUN
eurjchem-1358	36	18	d	d	NOUN
eurjchem-1358	36	19	was	be	AUX
eurjchem-1358	36	20	successful	successful	ADJ
eurjchem-1358	36	21	preparation	preparation	NOUN
eurjchem-1358	36	22	.	.	PUNCT
eurjchem-1358	37	1	d	d	NOUN
eurjchem-1358	37	2	in	in	ADP
eurjchem-1358	37	3	literatures	literature	NOUN
eurjchem-1358	37	4	osage	osage	NOUN
eurjchem-1358	37	5	forms	form	NOUN
eurjchem-1358	37	6	or	or	CCONJ
eurjchem-1358	37	7	n	n	CCONJ
eurjchem-1358	37	8	[	[	X
eurjchem-1358	37	9	9,10	9,10	NUM
eurjchem-1358	37	10	]	]	PUNCT
eurjchem-1358	37	11	,	,	PUNCT
eurjchem-1358	37	12	lc‐ms	lc‐ms	PROPN
eurjchem-1358	37	13	determined	determine	VERB
eurjchem-1358	37	14	in	in	ADP
eurjchem-1358	37	15	electrophoresis	electrophoresis	NOUN
eurjchem-1358	37	16	(	(	PUNCT
eurjchem-1358	37	17	a	a	PRON
eurjchem-1358	37	18	)	)	PUNCT
eurjchem-1358	37	19	product	product	NOUN
eurjchem-1358	37	20	paba	paba	NOUN
eurjchem-1358	37	21	(	(	PUNCT
eurjchem-1358	37	22	b	b	NOUN
eurjchem-1358	37	23	)	)	PUNCT
eurjchem-1358	37	24	.	.	PUNCT
eurjchem-1358	38	1	ad	ad	NOUN
eurjchem-1358	38	2	its	its	PRON
eurjchem-1358	38	3	nd	nd	NOUN
eurjchem-1358	38	4	on	on	ADP
eurjchem-1358	38	5	fer	fer	PROPN
eurjchem-1358	38	6	ate	eat	VERB
eurjchem-1358	38	7	on	on	ADP
eurjchem-1358	38	8	ge	ge	PROPN
eurjchem-1358	38	9	oq	oq	PROPN
eurjchem-1358	38	10	a	a	PROPN
eurjchem-1358	38	11	,	,	PUNCT
eurjchem-1358	38	12	lly	lly	ADV
eurjchem-1358	38	13	s	s	VERB
eurjchem-1358	38	14	r	r	NOUN
eurjchem-1358	38	15	s	s	X
eurjchem-1358	38	16	n	n	NOUN
eurjchem-1358	38	17	s	s	NUM
eurjchem-1358	38	18	98	98	NUM
eurjchem-1358	38	19	otilonium	otilonium	NOUN
eurjchem-1358	38	20	readily	readily	ADV
eurjchem-1358	38	21	und	und	ADJ
eurjchem-1358	38	22	benzamido)b	benzamido)b	X
eurjchem-1358	38	23	molecule	molecule	NOUN
eurjchem-1358	39	1	[	[	PUNCT
eurjchem-1358	39	2	1	1	NUM
eurjchem-1358	39	3	hydrolysis	hydrolysis	NOUN
eurjchem-1358	39	4	to	to	ADP
eurjchem-1358	39	5	one	one	NUM
eurjchem-1358	39	6	of	of	ADP
eurjchem-1358	39	7	the	the	DET
eurjchem-1358	39	8	de	de	PROPN
eurjchem-1358	39	9	present	present	PROPN
eurjchem-1358	39	10	wor	wor	PROPN
eurjchem-1358	39	11	stability‐indi	stability‐indi	PUNCT
eurjchem-1358	39	12	nation	nation	NOUN
eurjchem-1358	39	13	of	of	ADP
eurjchem-1358	39	14	o	o	PROPN
eurjchem-1358	39	15	pharmaceuti	pharmaceuti	NOUN
eurjchem-1358	39	16	2	2	NUM
eurjchem-1358	39	17	.	.	PUNCT
eurjchem-1358	39	18	experime	experime	PROPN
eurjchem-1358	39	19	2.1	2.1	NUM
eurjchem-1358	39	20	.	.	PUNCT
eurjchem-1358	40	1	instrum	instrum	INTJ
eurjchem-1358	40	2	an	an	DET
eurjchem-1358	40	3	agile	agile	ADJ
eurjchem-1358	40	4	vacuum	vacuum	NOUN
eurjchem-1358	40	5	dega	dega	PROPN
eurjchem-1358	40	6	detector	detector	NOUN
eurjchem-1358	40	7	was	be	AUX
eurjchem-1358	40	8	waters	water	NOUN
eurjchem-1358	40	9	atlan	atlan	PROPN
eurjchem-1358	40	10	processor	processor	PROPN
eurjchem-1358	40	11	m	m	PROPN
eurjchem-1358	40	12	vortex	vortex	NOUN
eurjchem-1358	40	13	mixer	mixer	NOUN
eurjchem-1358	40	14	2.2	2.2	NUM
eurjchem-1358	40	15	.	.	PUNCT
eurjchem-1358	41	1	reagent	reagent	ADJ
eurjchem-1358	41	2	all	all	DET
eurjchem-1358	41	3	chem	chem	NOUN
eurjchem-1358	41	4	grade	grade	NOUN
eurjchem-1358	41	5	.	.	PUNCT
eurjchem-1358	42	1	ob	ob	X
eurjchem-1358	42	2	(	(	PUNCT
eurjchem-1358	42	3	egypt	egypt	PROPN
eurjchem-1358	42	4	.	.	PUNCT
eurjchem-1358	43	1	p‐am	p‐am	PROPN
eurjchem-1358	43	2	buffer	buffer	NOUN
eurjchem-1358	43	3	analyt	analyt	ADJ
eurjchem-1358	43	4	acetonitrile	acetonitrile	ADJ
eurjchem-1358	43	5	scientific	scientific	NOUN
eurjchem-1358	43	6	,	,	PUNCT
eurjchem-1358	43	7	uk	uk	PROPN
eurjchem-1358	43	8	40	40	NUM
eurjchem-1358	43	9	mg	mg	NOUN
eurjchem-1358	43	10	ob	ob	ADP
eurjchem-1358	43	11	w	w	NOUN
eurjchem-1358	43	12	water	water	NOUN
eurjchem-1358	43	13	was	be	AUX
eurjchem-1358	43	14	u.s.a	u.s.a	NOUN
eurjchem-1358	43	15	.	.	PUNCT
eurjchem-1358	43	16	2.3	2.3	NUM
eurjchem-1358	43	17	.	.	PUNCT
eurjchem-1358	44	1	chroma	chroma	PROPN
eurjchem-1358	44	2	chromat	chromat	NOUN
eurjchem-1358	44	3	atlantis	atlantis	PROPN
eurjchem-1358	44	4	c18	c18	PROPN
eurjchem-1358	44	5	isocratic	isocratic	PROPN
eurjchem-1358	44	6	elut	elut	PROPN
eurjchem-1358	44	7	ammonium	ammonium	NOUN
eurjchem-1358	44	8	acetonitrile	acetonitrile	NOUN
eurjchem-1358	44	9	through	through	ADP
eurjchem-1358	44	10	the	the	DET
eurjchem-1358	44	11	performed	perform	VERB
eurjchem-1358	44	12	a	a	DET
eurjchem-1358	44	13	detection	detection	NOUN
eurjchem-1358	44	14	wa	wa	ADP
eurjchem-1358	44	15	2	2	NUM
eurjchem-1358	44	16	µl	µl	NOUN
eurjchem-1358	44	17	.	.	PUNCT
eurjchem-1358	44	18	2.4	2.4	NUM
eurjchem-1358	44	19	.	.	PUNCT
eurjchem-1358	45	1	prepara	prepara	PROPN
eurjchem-1358	45	2	accurate	accurate	ADJ
eurjchem-1358	45	3	ml	ml	NOUN
eurjchem-1358	45	4	volumet	volumet	ADJ
eurjchem-1358	45	5	volume	volume	NOUN
eurjchem-1358	45	6	with	with	ADP
eurjchem-1358	45	7	2.4.1	2.4.1	NUM
eurjchem-1358	45	8	.	.	PUNCT
eurjchem-1358	46	1	prepa	prepa	NOUN
eurjchem-1358	46	2	five	five	NUM
eurjchem-1358	46	3	ml	ml	NOUN
eurjchem-1358	46	4	volumetric	volumetric	NOUN
eurjchem-1358	46	5	f	f	PROPN
eurjchem-1358	46	6	acetonitrile	acetonitrile	NOUN
eurjchem-1358	46	7	(	(	PUNCT
eurjchem-1358	46	8	2.4.2	2.4.2	NUM
eurjchem-1358	46	9	.	.	PUNCT
eurjchem-1358	47	1	prepa	prepa	PROPN
eurjchem-1358	47	2	accurate	accurate	ADJ
eurjchem-1358	47	3	25	25	NUM
eurjchem-1358	47	4	ml	ml	NOUN
eurjchem-1358	47	5	volum	volum	NOUN
eurjchem-1358	47	6	volume	volume	NOUN
eurjchem-1358	47	7	with	with	ADP
eurjchem-1358	47	8	2.4.3	2.4.3	NUM
eurjchem-1358	47	9	.	.	PUNCT
eurjchem-1358	48	1	prepa	prepa	NOUN
eurjchem-1358	48	2	five	five	NUM
eurjchem-1358	48	3	ml	ml	NOUN
eurjchem-1358	48	4	volumetric	volumetric	NOUN
eurjchem-1358	48	5	f	f	PROPN
eurjchem-1358	48	6	acetonitrile	acetonitrile	NOUN
eurjchem-1358	48	7	(	(	PUNCT
eurjchem-1358	48	8	2.5	2.5	NUM
eurjchem-1358	48	9	.	.	PUNCT
eurjchem-1358	49	1	sample	sample	NOUN
eurjchem-1358	49	2	ten	ten	NUM
eurjchem-1358	49	3	sp	sp	ADP
eurjchem-1358	49	4	weighted	weight	VERB
eurjchem-1358	49	5	,	,	PUNCT
eurjchem-1358	49	6	cr	cr	PROPN
eurjchem-1358	49	7	m	m	PROPN
eurjchem-1358	49	8	bromide	bromide	PROPN
eurjchem-1358	49	9	de	de	X
eurjchem-1358	49	10	derwent	derwent	PROPN
eurjchem-1358	49	11	hydr	hydr	NOUN
eurjchem-1358	49	12	benzoic	benzoic	NOUN
eurjchem-1358	49	13	acid	acid	NOUN
eurjchem-1358	49	14	t	t	PROPN
eurjchem-1358	49	15	8	8	NUM
eurjchem-1358	49	16	]	]	PUNCT
eurjchem-1358	49	17	,	,	PUNCT
eurjchem-1358	49	18	and	and	CCONJ
eurjchem-1358	49	19	the	the	DET
eurjchem-1358	49	20	se	se	PROPN
eurjchem-1358	49	21	o	o	X
eurjchem-1358	49	22	amine	amine	NOUN
eurjchem-1358	50	1	[	[	X
eurjchem-1358	50	2	19	19	NUM
eurjchem-1358	50	3	]	]	PUNCT
eurjchem-1358	50	4	.	.	PUNCT
eurjchem-1358	51	1	t	t	PROPN
eurjchem-1358	51	2	egraded	egrade	VERB
eurjchem-1358	51	3	produc	produc	PROPN
eurjchem-1358	51	4	rk	rk	PROPN
eurjchem-1358	51	5	aimed	aim	VERB
eurjchem-1358	51	6	to	to	ADP
eurjchem-1358	51	7	de	de	X
eurjchem-1358	51	8	icating	icating	NOUN
eurjchem-1358	51	9	method	method	NOUN
eurjchem-1358	51	10	ob	ob	ADP
eurjchem-1358	51	11	and	and	CCONJ
eurjchem-1358	51	12	paba	paba	PROPN
eurjchem-1358	51	13	ical	ical	ADJ
eurjchem-1358	51	14	preparation	preparation	NOUN
eurjchem-1358	51	15	ental	ental	ADJ
eurjchem-1358	51	16	mentation	mentation	NOUN
eurjchem-1358	51	17	ent	ent	PROPN
eurjchem-1358	51	18	1260	1260	NUM
eurjchem-1358	51	19	hplc	hplc	PROPN
eurjchem-1358	51	20	asser	asser	PROPN
eurjchem-1358	51	21	,	,	PUNCT
eurjchem-1358	52	1	quaterna	quaterna	PROPN
eurjchem-1358	52	2	s	s	PRON
eurjchem-1358	52	3	used	use	VERB
eurjchem-1358	52	4	.	.	PUNCT
eurjchem-1358	53	1	separat	separat	PROPN
eurjchem-1358	53	2	ntis	ntis	PROPN
eurjchem-1358	53	3	c18	c18	PROPN
eurjchem-1358	53	4	column	column	PROPN
eurjchem-1358	53	5	model	model	PROPN
eurjchem-1358	53	6	kbk	kbk	PROPN
eurjchem-1358	53	7	420	420	NUM
eurjchem-1358	53	8	r	r	NOUN
eurjchem-1358	53	9	(	(	PUNCT
eurjchem-1358	53	10	berlin	berlin	PROPN
eurjchem-1358	53	11	)	)	PUNCT
eurjchem-1358	53	12	were	be	AUX
eurjchem-1358	53	13	ts	ts	ADP
eurjchem-1358	53	14	and	and	CCONJ
eurjchem-1358	53	15	referenc	referenc	ADJ
eurjchem-1358	53	16	micals	mical	NOUN
eurjchem-1358	53	17	and	and	CCONJ
eurjchem-1358	53	18	reage	reage	NOUN
eurjchem-1358	53	19	>	>	PUNCT
eurjchem-1358	53	20	99	99	NUM
eurjchem-1358	53	21	%	%	NOUN
eurjchem-1358	53	22	)	)	PUNCT
eurjchem-1358	53	23	was	be	AUX
eurjchem-1358	53	24	ki	ki	PROPN
eurjchem-1358	53	25	minobenzoic	minobenzoic	PROPN
eurjchem-1358	53	26	aci	aci	PROPN
eurjchem-1358	53	27	tical	tical	PROPN
eurjchem-1358	53	28	grade	grade	NOUN
eurjchem-1358	53	29	wer	wer	NOUN
eurjchem-1358	53	30	(	(	PUNCT
eurjchem-1358	53	31	hplc	hplc	NOUN
eurjchem-1358	53	32	grade	grade	PROPN
eurjchem-1358	53	33	k.	k.	PROPN
eurjchem-1358	53	34	spasmomen	spasmomen	PROPN
eurjchem-1358	53	35	®	®	PROPN
eurjchem-1358	53	36	was	be	AUX
eurjchem-1358	53	37	purchased	purchase	VERB
eurjchem-1358	53	38	produced	produce	VERB
eurjchem-1358	53	39	in‐h	in‐h	NUM
eurjchem-1358	53	40	atographic	atographic	ADJ
eurjchem-1358	53	41	cond	cond	NOUN
eurjchem-1358	53	42	tographic	tographic	ADJ
eurjchem-1358	53	43	sepa	sepa	NOUN
eurjchem-1358	53	44	8	8	NUM
eurjchem-1358	53	45	column	column	NOUN
eurjchem-1358	53	46	(	(	PUNCT
eurjchem-1358	53	47	4.6	4.6	NUM
eurjchem-1358	53	48	tion	tion	NOUN
eurjchem-1358	53	49	based	base	VERB
eurjchem-1358	53	50	on	on	ADP
eurjchem-1358	53	51	a	a	DET
eurjchem-1358	53	52	acetate	acetate	NOUN
eurjchem-1358	53	53	buffer	buffer	NOUN
eurjchem-1358	53	54	(	(	PUNCT
eurjchem-1358	53	55	30:70	30:70	NUM
eurjchem-1358	53	56	,	,	PUNCT
eurjchem-1358	53	57	v	v	NOUN
eurjchem-1358	53	58	:	:	PUNCT
eurjchem-1358	53	59	v	v	NOUN
eurjchem-1358	53	60	)	)	PUNCT
eurjchem-1358	53	61	.	.	PUNCT
eurjchem-1358	54	1	column	column	NOUN
eurjchem-1358	54	2	at	at	ADP
eurjchem-1358	54	3	a	a	DET
eurjchem-1358	54	4	flo	flo	NOUN
eurjchem-1358	54	5	at	at	ADP
eurjchem-1358	54	6	controlled	control	VERB
eurjchem-1358	54	7	as	as	SCONJ
eurjchem-1358	54	8	carried	carry	VERB
eurjchem-1358	54	9	out	out	ADP
eurjchem-1358	54	10	a	a	DET
eurjchem-1358	54	11	ation	ation	NOUN
eurjchem-1358	54	12	of	of	ADP
eurjchem-1358	54	13	ob	ob	PROPN
eurjchem-1358	54	14	stan	stan	PROPN
eurjchem-1358	54	15	ely	ely	PROPN
eurjchem-1358	54	16	weight	weight	PROPN
eurjchem-1358	54	17	25	25	NUM
eurjchem-1358	54	18	m	m	NOUN
eurjchem-1358	54	19	tric	tric	ADJ
eurjchem-1358	54	20	flask	flask	NOUN
eurjchem-1358	54	21	and	and	CCONJ
eurjchem-1358	54	22	d	d	NOUN
eurjchem-1358	54	23	acetonitrile	acetonitrile	NOUN
eurjchem-1358	54	24	(	(	PUNCT
eurjchem-1358	54	25	1	1	NUM
eurjchem-1358	54	26	ration	ration	NOUN
eurjchem-1358	54	27	of	of	ADP
eurjchem-1358	54	28	ob	ob	NOUN
eurjchem-1358	54	29	w	w	PROPN
eurjchem-1358	54	30	of	of	ADP
eurjchem-1358	54	31	ob	ob	NOUN
eurjchem-1358	54	32	stock	stock	NOUN
eurjchem-1358	54	33	so	so	ADV
eurjchem-1358	54	34	flask	flask	NOUN
eurjchem-1358	54	35	;	;	PUNCT
eurjchem-1358	54	36	the	the	DET
eurjchem-1358	54	37	volu	volu	PROPN
eurjchem-1358	54	38	(	(	PUNCT
eurjchem-1358	54	39	100	100	NUM
eurjchem-1358	54	40	μg	μg	NOUN
eurjchem-1358	54	41	/	/	SYM
eurjchem-1358	54	42	ml	ml	NOUN
eurjchem-1358	54	43	)	)	PUNCT
eurjchem-1358	54	44	.	.	PUNCT
eurjchem-1358	55	1	ration	ration	NOUN
eurjchem-1358	55	2	of	of	ADP
eurjchem-1358	55	3	paba	paba	PROPN
eurjchem-1358	55	4	ely	ely	ADV
eurjchem-1358	55	5	weight	weight	VERB
eurjchem-1358	55	6	25	25	NUM
eurjchem-1358	55	7	m	m	NOUN
eurjchem-1358	55	8	metric	metric	ADJ
eurjchem-1358	55	9	flask	flask	NOUN
eurjchem-1358	55	10	and	and	CCONJ
eurjchem-1358	55	11	acetonitrile	acetonitrile	ADJ
eurjchem-1358	55	12	(	(	PUNCT
eurjchem-1358	55	13	1	1	NUM
eurjchem-1358	55	14	ration	ration	NOUN
eurjchem-1358	55	15	of	of	ADP
eurjchem-1358	55	16	paba	paba	NOUN
eurjchem-1358	55	17	of	of	ADP
eurjchem-1358	55	18	paba	paba	PROPN
eurjchem-1358	55	19	stock	stock	PROPN
eurjchem-1358	55	20	s	s	PART
eurjchem-1358	55	21	flask	flask	NOUN
eurjchem-1358	55	22	;	;	PUNCT
eurjchem-1358	55	23	the	the	DET
eurjchem-1358	55	24	volu	volu	PROPN
eurjchem-1358	55	25	(	(	PUNCT
eurjchem-1358	55	26	100	100	NUM
eurjchem-1358	55	27	μg	μg	NOUN
eurjchem-1358	55	28	/	/	SYM
eurjchem-1358	55	29	ml	ml	NOUN
eurjchem-1358	55	30	)	)	PUNCT
eurjchem-1358	55	31	.	.	PUNCT
eurjchem-1358	56	1	solution	solution	NOUN
eurjchem-1358	56	2	prepa	prepa	PROPN
eurjchem-1358	56	3	asmomen	asmoman	NOUN
eurjchem-1358	56	4	®	®	NOUN
eurjchem-1358	56	5	4	4	NUM
eurjchem-1358	56	6	ushed	ushe	VERB
eurjchem-1358	56	7	then	then	ADV
eurjchem-1358	56	8	mix	mix	VERB
eurjchem-1358	56	9	el‐k	el‐k	PROPN
eurjchem-1358	56	10	egraded	egrade	VERB
eurjchem-1358	56	11	at	at	ADP
eurjchem-1358	56	12	roo	roo	PROPN
eurjchem-1358	56	13	rolysis	rolysis	PROPN
eurjchem-1358	56	14	to	to	ADP
eurjchem-1358	56	15	yi	yi	VERB
eurjchem-1358	56	16	through	through	ADP
eurjchem-1358	56	17	the	the	DET
eurjchem-1358	56	18	e	e	NOUN
eurjchem-1358	56	19	econdary	econdary	ADJ
eurjchem-1358	56	20	amid	amid	ADP
eurjchem-1358	56	21	therefore	therefore	ADV
eurjchem-1358	56	22	paba	paba	PROPN
eurjchem-1358	56	23	cts	ct	NOUN
eurjchem-1358	56	24	of	of	ADP
eurjchem-1358	56	25	ob	ob	NOUN
eurjchem-1358	56	26	from	from	ADP
eurjchem-1358	56	27	evelop	evelop	NOUN
eurjchem-1358	56	28	a	a	PRON
eurjchem-1358	56	29	fast	fast	NOUN
eurjchem-1358	56	30	,	,	PUNCT
eurjchem-1358	56	31	r	r	NOUN
eurjchem-1358	56	32	d	d	PROPN
eurjchem-1358	56	33	for	for	ADP
eurjchem-1358	56	34	the	the	DET
eurjchem-1358	56	35	sim	sim	NOUN
eurjchem-1358	56	36	(	(	PUNCT
eurjchem-1358	56	37	figure	figure	NOUN
eurjchem-1358	56	38	1	1	NUM
eurjchem-1358	56	39	)	)	PUNCT
eurjchem-1358	56	40	in	in	ADP
eurjchem-1358	56	41	n.	n.	NOUN
eurjchem-1358	56	42	system	system	NOUN
eurjchem-1358	56	43	(	(	PUNCT
eurjchem-1358	56	44	germ	germ	NOUN
eurjchem-1358	56	45	ary‐pump	ary‐pump	NOUN
eurjchem-1358	56	46	,	,	PUNCT
eurjchem-1358	56	47	colum	colum	NOUN
eurjchem-1358	56	48	ion	ion	NOUN
eurjchem-1358	56	49	and	and	CCONJ
eurjchem-1358	56	50	quantit	quantit	NOUN
eurjchem-1358	56	51	n	n	CCONJ
eurjchem-1358	56	52	(	(	PUNCT
eurjchem-1358	56	53	4.6	4.6	NUM
eurjchem-1358	56	54	×	×	NOUN
eurjchem-1358	56	55	150	150	NUM
eurjchem-1358	56	56	m	m	NOUN
eurjchem-1358	56	57	00	00	NUM
eurjchem-1358	56	58	(	(	PUNCT
eurjchem-1358	56	59	germany	germany	PROPN
eurjchem-1358	56	60	)	)	PUNCT
eurjchem-1358	56	61	a	a	DET
eurjchem-1358	56	62	used	use	VERB
eurjchem-1358	56	63	.	.	PUNCT
eurjchem-1358	57	1	ce	ce	PROPN
eurjchem-1358	57	2	samples	sample	NOUN
eurjchem-1358	57	3	ents	ent	NOUN
eurjchem-1358	57	4	used	use	VERB
eurjchem-1358	57	5	were	be	AUX
eurjchem-1358	57	6	o	o	PROPN
eurjchem-1358	57	7	indly	indly	ADV
eurjchem-1358	57	8	provided	provide	VERB
eurjchem-1358	57	9	i	i	PROPN
eurjchem-1358	57	10	d	d	PROPN
eurjchem-1358	57	11	(	(	PUNCT
eurjchem-1358	57	12	99	99	NUM
eurjchem-1358	57	13	%	%	NOUN
eurjchem-1358	57	14	)	)	PUNCT
eurjchem-1358	57	15	and	and	CCONJ
eurjchem-1358	57	16	re	re	VERB
eurjchem-1358	57	17	purchased	purchase	VERB
eurjchem-1358	57	18	fr	fr	PROPN
eurjchem-1358	57	19	e	e	NOUN
eurjchem-1358	57	20	)	)	PUNCT
eurjchem-1358	57	21	was	be	AUX
eurjchem-1358	57	22	purch	purch	ADJ
eurjchem-1358	57	23	®	®	NOUN
eurjchem-1358	57	24	40	40	NUM
eurjchem-1358	57	25	mg	mg	NOUN
eurjchem-1358	57	26	tablet	tablet	NOUN
eurjchem-1358	57	27	n	n	PROPN
eurjchem-1358	57	28	from	from	ADP
eurjchem-1358	57	29	a	a	DET
eurjchem-1358	57	30	local	local	ADJ
eurjchem-1358	57	31	p	p	NOUN
eurjchem-1358	57	32	house	house	NOUN
eurjchem-1358	57	33	by	by	ADP
eurjchem-1358	57	34	barn	barn	ADJ
eurjchem-1358	57	35	ditions	dition	NOUN
eurjchem-1358	57	36	aration	aration	NOUN
eurjchem-1358	57	37	was	be	AUX
eurjchem-1358	57	38	a	a	DET
eurjchem-1358	57	39	×	×	NOUN
eurjchem-1358	57	40	150	150	NUM
eurjchem-1358	57	41	mm	mm	NOUN
eurjchem-1358	57	42	,	,	PUNCT
eurjchem-1358	57	43	a	a	DET
eurjchem-1358	57	44	mobile	mobile	ADJ
eurjchem-1358	57	45	phase	phase	NOUN
eurjchem-1358	57	46	(	(	PUNCT
eurjchem-1358	57	47	ph	ph	NOUN
eurjchem-1358	57	48	=	=	SYM
eurjchem-1358	57	49	2.35	2.35	NUM
eurjchem-1358	57	50	)	)	PUNCT
eurjchem-1358	57	51	the	the	DET
eurjchem-1358	57	52	mobile	mobile	NOUN
eurjchem-1358	57	53	p	p	NOUN
eurjchem-1358	57	54	w	w	NOUN
eurjchem-1358	57	55	rate	rate	NOUN
eurjchem-1358	57	56	of	of	ADP
eurjchem-1358	57	57	0.8	0.8	NUM
eurjchem-1358	57	58	m	m	NOUN
eurjchem-1358	57	59	column	column	NOUN
eurjchem-1358	57	60	temp	temp	NOUN
eurjchem-1358	57	61	t	t	PROPN
eurjchem-1358	57	62	290	290	NUM
eurjchem-1358	57	63	nm	nm	NOUN
eurjchem-1358	57	64	.	.	PUNCT
eurjchem-1358	58	1	the	the	DET
eurjchem-1358	58	2	i	i	PRON
eurjchem-1358	58	3	ndard	ndard	VERB
eurjchem-1358	58	4	stock	stock	NOUN
eurjchem-1358	58	5	so	so	SCONJ
eurjchem-1358	58	6	mg	mg	PROPN
eurjchem-1358	58	7	of	of	ADP
eurjchem-1358	58	8	ob	ob	PRON
eurjchem-1358	58	9	was	be	AUX
eurjchem-1358	58	10	t	t	NOUN
eurjchem-1358	58	11	dissolved	dissolve	VERB
eurjchem-1358	58	12	in	in	ADP
eurjchem-1358	58	13	an	an	DET
eurjchem-1358	58	14	mg	mg	PROPN
eurjchem-1358	58	15	/	/	SYM
eurjchem-1358	58	16	ml	ml	NOUN
eurjchem-1358	58	17	)	)	PUNCT
eurjchem-1358	58	18	.	.	PUNCT
eurjchem-1358	59	1	working	working	NOUN
eurjchem-1358	59	2	solutio	solutio	PROPN
eurjchem-1358	59	3	olution	olution	NOUN
eurjchem-1358	59	4	was	be	AUX
eurjchem-1358	59	5	tra	tra	PROPN
eurjchem-1358	59	6	ume	ume	PROPN
eurjchem-1358	59	7	was	be	AUX
eurjchem-1358	59	8	comp	comp	NOUN
eurjchem-1358	59	9	a	a	DET
eurjchem-1358	59	10	stock	stock	NOUN
eurjchem-1358	59	11	solution	solution	NOUN
eurjchem-1358	59	12	mg	mg	ADP
eurjchem-1358	59	13	of	of	ADP
eurjchem-1358	59	14	paba	paba	PROPN
eurjchem-1358	60	1	wa	wa	PROPN
eurjchem-1358	60	2	d	d	PROPN
eurjchem-1358	60	3	dissolved	dissolve	VERB
eurjchem-1358	60	4	in	in	ADP
eurjchem-1358	60	5	a	a	DET
eurjchem-1358	60	6	mg	mg	PROPN
eurjchem-1358	60	7	/	/	SYM
eurjchem-1358	60	8	ml	ml	NOUN
eurjchem-1358	60	9	)	)	PUNCT
eurjchem-1358	60	10	.	.	PUNCT
eurjchem-1358	61	1	a	a	DET
eurjchem-1358	61	2	working	working	NOUN
eurjchem-1358	61	3	solu	solu	PROPN
eurjchem-1358	61	4	solution	solution	NOUN
eurjchem-1358	61	5	was	be	AUX
eurjchem-1358	61	6	tr	tr	VERB
eurjchem-1358	61	7	ume	ume	ADJ
eurjchem-1358	61	8	was	be	AUX
eurjchem-1358	61	9	comp	comp	NOUN
eurjchem-1358	61	10	aration	aration	NOUN
eurjchem-1358	61	11	40	40	NUM
eurjchem-1358	61	12	mg	mg	PROPN
eurjchem-1358	61	13	tablet	tablet	PROPN
eurjchem-1358	61	14	xed	xed	PROPN
eurjchem-1358	61	15	well	well	ADV
eurjchem-1358	61	16	.	.	PUNCT
eurjchem-1358	62	1	accur	accur	PROPN
eurjchem-1358	62	2	kerdawy	kerdawy	PROPN
eurjchem-1358	62	3	et	et	PROPN
eurjchem-1358	62	4	al	al	PROPN
eurjchem-1358	62	5	.	.	PUNCT
eurjchem-1358	62	6	/	/	PUNCT
eurjchem-1358	63	1	e	e	X
eurjchem-1358	63	2	m	m	PROPN
eurjchem-1358	63	3	temperatur	temperatur	PROPN
eurjchem-1358	63	4	eld	eld	PROPN
eurjchem-1358	63	5	4‐(2‐(octy	4‐(2‐(octy	PROPN
eurjchem-1358	63	6	ester	ester	NOUN
eurjchem-1358	63	7	group	group	NOUN
eurjchem-1358	63	8	in	in	ADP
eurjchem-1358	63	9	de	de	PROPN
eurjchem-1358	63	10	group	group	PROPN
eurjchem-1358	63	11	unde	unde	PROPN
eurjchem-1358	63	12	a	a	PRON
eurjchem-1358	63	13	is	be	AUX
eurjchem-1358	63	14	predicted	predict	VERB
eurjchem-1358	63	15	both	both	PRON
eurjchem-1358	63	16	hydrolysi	hydrolysi	PROPN
eurjchem-1358	63	17	obust	obust	NOUN
eurjchem-1358	63	18	and	and	CCONJ
eurjchem-1358	63	19	econ	econ	PROPN
eurjchem-1358	63	20	multaneous	multaneous	PROPN
eurjchem-1358	63	21	det	det	PROPN
eurjchem-1358	63	22	n	n	CCONJ
eurjchem-1358	63	23	bulk	bulk	ADJ
eurjchem-1358	63	24	powder	powder	NOUN
eurjchem-1358	63	25	many	many	ADJ
eurjchem-1358	63	26	)	)	PUNCT
eurjchem-1358	63	27	,	,	PUNCT
eurjchem-1358	63	28	equipped	equip	VERB
eurjchem-1358	63	29	mn	mn	PROPN
eurjchem-1358	63	30	oven	oven	NOUN
eurjchem-1358	63	31	and	and	CCONJ
eurjchem-1358	63	32	u	u	NOUN
eurjchem-1358	63	33	tation	tation	NOUN
eurjchem-1358	63	34	were	be	AUX
eurjchem-1358	63	35	ma	ma	PROPN
eurjchem-1358	63	36	mm	mm	PROPN
eurjchem-1358	63	37	,	,	PUNCT
eurjchem-1358	63	38	5	5	NUM
eurjchem-1358	63	39	µm	µm	NOUN
eurjchem-1358	63	40	)	)	PUNCT
eurjchem-1358	63	41	.	.	PUNCT
eurjchem-1358	64	1	ultra	ultra	ADJ
eurjchem-1358	64	2	and	and	CCONJ
eurjchem-1358	64	3	scilogex	scilogex	NOUN
eurjchem-1358	64	4	of	of	ADP
eurjchem-1358	64	5	analytical	analytical	ADJ
eurjchem-1358	64	6	or	or	CCONJ
eurjchem-1358	64	7	d	d	NOUN
eurjchem-1358	64	8	by	by	ADP
eurjchem-1358	64	9	minapharm	minapharm	NOUN
eurjchem-1358	64	10	ammonium	ammonium	NOUN
eurjchem-1358	64	11	a	a	DET
eurjchem-1358	64	12	om	om	PROPN
eurjchem-1358	64	13	merck	merck	PROPN
eurjchem-1358	64	14	,	,	PUNCT
eurjchem-1358	64	15	ger	ger	NOUN
eurjchem-1358	64	16	hased	hase	VERB
eurjchem-1358	64	17	from	from	ADP
eurjchem-1358	64	18	f	f	PROPN
eurjchem-1358	64	19	nominally	nominally	ADV
eurjchem-1358	64	20	conta	conta	PROPN
eurjchem-1358	64	21	pharmacy	pharmacy	PROPN
eurjchem-1358	64	22	.	.	PUNCT
eurjchem-1358	65	1	deio	deio	PROPN
eurjchem-1358	65	2	nstead	nstead	PROPN
eurjchem-1358	65	3	diamond	diamond	PROPN
eurjchem-1358	65	4	achieved	achieve	VERB
eurjchem-1358	65	5	on	on	ADP
eurjchem-1358	65	6	w	w	PROPN
eurjchem-1358	65	7	5	5	NUM
eurjchem-1358	65	8	µm	µm	NOUN
eurjchem-1358	65	9	)	)	PUNCT
eurjchem-1358	65	10	by	by	ADP
eurjchem-1358	65	11	app	app	PROPN
eurjchem-1358	65	12	e	e	NOUN
eurjchem-1358	65	13	consisting	consist	VERB
eurjchem-1358	65	14	of	of	ADP
eurjchem-1358	65	15	contain	contain	NOUN
eurjchem-1358	65	16	0.05	0.05	NUM
eurjchem-1358	65	17	%	%	NOUN
eurjchem-1358	65	18	phase	phase	NOUN
eurjchem-1358	65	19	was	be	AUX
eurjchem-1358	65	20	pu	pu	PROPN
eurjchem-1358	65	21	ml	ml	PROPN
eurjchem-1358	65	22	/	/	SYM
eurjchem-1358	65	23	min	min	PROPN
eurjchem-1358	65	24	.	.	PROPN
eurjchem-1358	65	25	analysi	analysi	NOUN
eurjchem-1358	65	26	erature	erature	NOUN
eurjchem-1358	65	27	25	25	NUM
eurjchem-1358	65	28	°	°	NOUN
eurjchem-1358	65	29	c	c	NOUN
eurjchem-1358	65	30	injection	injection	NOUN
eurjchem-1358	65	31	volum	volum	NOUN
eurjchem-1358	65	32	olution	olution	NOUN
eurjchem-1358	65	33	transferred	transfer	VERB
eurjchem-1358	65	34	into	into	ADP
eurjchem-1358	65	35	nd	nd	ADV
eurjchem-1358	65	36	completed	complete	VERB
eurjchem-1358	65	37	t	t	NOUN
eurjchem-1358	65	38	n	n	CCONJ
eurjchem-1358	65	39	ansferred	ansferre	VERB
eurjchem-1358	65	40	to	to	ADP
eurjchem-1358	65	41	a	a	DET
eurjchem-1358	65	42	5	5	NUM
eurjchem-1358	65	43	pleted	plete	VERB
eurjchem-1358	65	44	to	to	PART
eurjchem-1358	65	45	mark	mark	VERB
eurjchem-1358	65	46	n	n	PRON
eurjchem-1358	65	47	as	as	ADV
eurjchem-1358	65	48	transferred	transfer	VERB
eurjchem-1358	65	49	and	and	CCONJ
eurjchem-1358	65	50	completed	complete	VERB
eurjchem-1358	65	51	tion	tion	NOUN
eurjchem-1358	65	52	ansferred	ansferre	VERB
eurjchem-1358	65	53	to	to	ADP
eurjchem-1358	65	54	a	a	DET
eurjchem-1358	65	55	5	5	NUM
eurjchem-1358	65	56	pleted	plete	VERB
eurjchem-1358	65	57	to	to	PART
eurjchem-1358	65	58	mark	mark	VERB
eurjchem-1358	65	59	ts	ts	PROPN
eurjchem-1358	65	60	were	be	AUX
eurjchem-1358	65	61	accu	accu	PROPN
eurjchem-1358	65	62	rately	rately	ADV
eurjchem-1358	65	63	weighed	weigh	VERB
eurjchem-1358	65	64	european	european	PROPN
eurjchem-1358	65	65	journa	journa	PROPN
eurjchem-1358	65	66	e	e	PROPN
eurjchem-1358	65	67	and	and	CCONJ
eurjchem-1358	65	68	yloxy	yloxy	PROPN
eurjchem-1358	65	69	)	)	PUNCT
eurjchem-1358	65	70	n	n	CCONJ
eurjchem-1358	65	71	the	the	DET
eurjchem-1358	65	72	rwent	rwent	NOUN
eurjchem-1358	65	73	to	to	PART
eurjchem-1358	65	74	be	be	AUX
eurjchem-1358	65	75	s.	s.	PROPN
eurjchem-1358	65	76	the	the	DET
eurjchem-1358	65	77	nomic	nomic	PROPN
eurjchem-1358	66	1	termi‐	termi‐	PROPN
eurjchem-1358	66	2	r	r	NOUN
eurjchem-1358	66	3	and	and	CCONJ
eurjchem-1358	66	4	d	d	NOUN
eurjchem-1358	66	5	with	with	ADP
eurjchem-1358	66	6	uv	uv	NOUN
eurjchem-1358	66	7	/	/	SYM
eurjchem-1358	66	8	vis	vis	X
eurjchem-1358	66	9	ade	ade	NOUN
eurjchem-1358	66	10	on	on	ADP
eurjchem-1358	66	11	asonic	asonic	ADJ
eurjchem-1358	66	12	mx‐s	mx‐s	ADJ
eurjchem-1358	66	13	hplc	hplc	NOUN
eurjchem-1358	66	14	m	m	VERB
eurjchem-1358	66	15	co	co	NOUN
eurjchem-1358	66	16	,	,	PUNCT
eurjchem-1358	66	17	cetate	cetate	VERB
eurjchem-1358	66	18	many	many	ADJ
eurjchem-1358	66	19	.	.	PUNCT
eurjchem-1358	67	1	fisher	fisher	PROPN
eurjchem-1358	67	2	aining	aining	PROPN
eurjchem-1358	67	3	onized	onize	VERB
eurjchem-1358	67	4	d	d	SYM
eurjchem-1358	67	5	ro	ro	PROPN
eurjchem-1358	67	6	,	,	PUNCT
eurjchem-1358	67	7	waters	water	NOUN
eurjchem-1358	67	8	plying	ply	VERB
eurjchem-1358	67	9	2	2	NUM
eurjchem-1358	67	10	mm	mm	NOUN
eurjchem-1358	67	11	%	%	NOUN
eurjchem-1358	67	12	tfa	tfa	NOUN
eurjchem-1358	67	13	:	:	PUNCT
eurjchem-1358	67	14	umped	umped	PROPN
eurjchem-1358	67	15	is	be	AUX
eurjchem-1358	67	16	was	be	AUX
eurjchem-1358	67	17	c	c	NOUN
eurjchem-1358	67	18	and	and	CCONJ
eurjchem-1358	67	19	me	i	PRON
eurjchem-1358	67	20	was	be	AUX
eurjchem-1358	67	21	o	o	PROPN
eurjchem-1358	67	22	a	a	DET
eurjchem-1358	67	23	25	25	NUM
eurjchem-1358	67	24	to	to	ADP
eurjchem-1358	67	25	the	the	DET
eurjchem-1358	67	26	50	50	NUM
eurjchem-1358	67	27	ml	ml	NOUN
eurjchem-1358	67	28	k	k	NOUN
eurjchem-1358	67	29	with	with	ADP
eurjchem-1358	67	30	into	into	ADP
eurjchem-1358	67	31	a	a	PRON
eurjchem-1358	67	32	to	to	ADP
eurjchem-1358	67	33	the	the	DET
eurjchem-1358	67	34	50	50	NUM
eurjchem-1358	67	35	ml	ml	NOUN
eurjchem-1358	67	36	k	k	NOUN
eurjchem-1358	67	37	with	with	ADP
eurjchem-1358	67	38	urately	urately	ADV
eurjchem-1358	67	39	128.1	128.1	NUM
eurjchem-1358	67	40	mg	mg	PROPN
eurjchem-1358	67	41	bro	bro	NOUN
eurjchem-1358	67	42	abo	abo	PROPN
eurjchem-1358	67	43	son	son	PROPN
eurjchem-1358	67	44	volu	volu	PROPN
eurjchem-1358	67	45	solu	solu	PROPN
eurjchem-1358	67	46	use	use	VERB
eurjchem-1358	67	47	2.6	2.6	NUM
eurjchem-1358	67	48	.	.	PUNCT
eurjchem-1358	67	49	2.6	2.6	NUM
eurjchem-1358	67	50	.	.	PUNCT
eurjchem-1358	68	1	tran	tran	PROPN
eurjchem-1358	68	2	volu	volu	PROPN
eurjchem-1358	68	3	solu	solu	PROPN
eurjchem-1358	68	4	ren	ren	PROPN
eurjchem-1358	68	5	into	into	ADP
eurjchem-1358	68	6	to	to	ADP
eurjchem-1358	68	7	v	v	NUM
eurjchem-1358	68	8	50	50	NUM
eurjchem-1358	68	9	inje	inje	NOUN
eurjchem-1358	68	10	incl	incl	NOUN
eurjchem-1358	68	11	dete	dete	PROPN
eurjchem-1358	68	12	obt	obt	PROPN
eurjchem-1358	68	13	con	con	PROPN
eurjchem-1358	68	14	2.6	2.6	NUM
eurjchem-1358	68	15	.	.	PUNCT
eurjchem-1358	69	1	usin	usin	PROPN
eurjchem-1358	69	2	5‐4	5‐4	PROPN
eurjchem-1358	69	3	2.6	2.6	NUM
eurjchem-1358	69	4	.	.	PUNCT
eurjchem-1358	70	1	pab	pab	NOUN
eurjchem-1358	70	2	for	for	ADP
eurjchem-1358	70	3	pre	pre	VERB
eurjchem-1358	70	4	and	and	CCONJ
eurjchem-1358	70	5	com	com	X
eurjchem-1358	70	6	con	con	PROPN
eurjchem-1358	70	7	eac	eac	PROPN
eurjchem-1358	70	8	figu	figu	PROPN
eurjchem-1358	70	9	labo	labo	PROPN
eurjchem-1358	70	10	2.6	2.6	NUM
eurjchem-1358	70	11	.	.	PUNCT
eurjchem-1358	71	1	dilu	dilu	PROPN
eurjchem-1358	71	2	trip	trip	NOUN
eurjchem-1358	71	3	calc	calc	NOUN
eurjchem-1358	71	4	figu	figu	PROPN
eurjchem-1358	71	5	sam	sam	PROPN
eurjchem-1358	71	6	al	al	PROPN
eurjchem-1358	71	7	of	of	ADP
eurjchem-1358	71	8	chemistry	chemistry	NOUN
eurjchem-1358	71	9	7	7	NUM
eurjchem-1358	71	10	of	of	ADP
eurjchem-1358	71	11	the	the	DET
eurjchem-1358	71	12	powde	powde	ADJ
eurjchem-1358	71	13	omide	omide	NOUN
eurjchem-1358	71	14	,	,	PUNCT
eurjchem-1358	71	15	were	be	AUX
eurjchem-1358	71	16	tra	tra	PROPN
eurjchem-1358	71	17	out	out	ADV
eurjchem-1358	71	18	30	30	NUM
eurjchem-1358	71	19	ml	ml	NOUN
eurjchem-1358	71	20	ac	ac	PROPN
eurjchem-1358	71	21	nicated	nicate	VERB
eurjchem-1358	71	22	for	for	ADP
eurjchem-1358	71	23	15	15	NUM
eurjchem-1358	71	24	m	m	NOUN
eurjchem-1358	71	25	ume	ume	NOUN
eurjchem-1358	71	26	was	be	AUX
eurjchem-1358	71	27	com	com	NOUN
eurjchem-1358	71	28	ution	ution	NOUN
eurjchem-1358	71	29	was	be	AUX
eurjchem-1358	71	30	filter	filter	NOUN
eurjchem-1358	71	31	ed	ed	NOUN
eurjchem-1358	71	32	as	as	ADP
eurjchem-1358	71	33	the	the	DET
eurjchem-1358	71	34	sample	sample	NOUN
eurjchem-1358	71	35	.	.	PUNCT
eurjchem-1358	72	1	procedure	procedure	NOUN
eurjchem-1358	72	2	.1	.1	PROPN
eurjchem-1358	72	3	.	.	PUNCT
eurjchem-1358	73	1	constructio	constructio	PROPN
eurjchem-1358	73	2	different	different	ADJ
eurjchem-1358	73	3	aliq	aliq	PROPN
eurjchem-1358	73	4	nsferred	nsferre	VERB
eurjchem-1358	73	5	into	into	ADP
eurjchem-1358	73	6	umes	ume	NOUN
eurjchem-1358	73	7	were	be	AUX
eurjchem-1358	73	8	co	co	NOUN
eurjchem-1358	73	9	utions	ution	NOUN
eurjchem-1358	73	10	containi	containi	PROPN
eurjchem-1358	73	11	t	t	PROPN
eurjchem-1358	73	12	aliquots	aliquot	NOUN
eurjchem-1358	73	13	from	from	ADP
eurjchem-1358	73	14	o	o	PROPN
eurjchem-1358	73	15	another	another	DET
eurjchem-1358	73	16	serie	serie	ADJ
eurjchem-1358	73	17	volumes	volume	NOUN
eurjchem-1358	73	18	with	with	ADP
eurjchem-1358	73	19	m	m	PROPN
eurjchem-1358	73	20	μg	μg	PROPN
eurjchem-1358	73	21	/	/	SYM
eurjchem-1358	73	22	ml	ml	NOUN
eurjchem-1358	73	23	paba	paba	PROPN
eurjchem-1358	73	24	.	.	PUNCT
eurjchem-1358	74	1	ected	ecte	VERB
eurjchem-1358	74	2	in	in	ADP
eurjchem-1358	74	3	triplica	triplica	NOUN
eurjchem-1358	74	4	luding	lude	VERB
eurjchem-1358	74	5	the	the	DET
eurjchem-1358	74	6	mo	mo	PROPN
eurjchem-1358	74	7	ection	ection	NOUN
eurjchem-1358	74	8	at	at	ADP
eurjchem-1358	74	9	290	290	NUM
eurjchem-1358	74	10	n	n	PRON
eurjchem-1358	74	11	ained	aine	VERB
eurjchem-1358	74	12	by	by	ADP
eurjchem-1358	74	13	plot	plot	NOUN
eurjchem-1358	74	14	ncentration	ncentration	NOUN
eurjchem-1358	74	15	(	(	PUNCT
eurjchem-1358	74	16	c	c	NOUN
eurjchem-1358	74	17	)	)	PUNCT
eurjchem-1358	74	18	.	.	PUNCT
eurjchem-1358	75	1	.2	.2	NUM
eurjchem-1358	75	2	.	.	PUNCT
eurjchem-1358	76	1	assay	assay	NOUN
eurjchem-1358	76	2	of	of	ADP
eurjchem-1358	76	3	ob	ob	ADP
eurjchem-1358	76	4	the	the	DET
eurjchem-1358	76	5	procedure	procedure	NOUN
eurjchem-1358	76	6	ng	ng	PROPN
eurjchem-1358	76	7	concentratio	concentratio	NOUN
eurjchem-1358	76	8	5	5	NUM
eurjchem-1358	76	9	μg	μg	PROPN
eurjchem-1358	76	10	/	/	SYM
eurjchem-1358	76	11	ml	ml	NOUN
eurjchem-1358	76	12	paba	paba	PROPN
eurjchem-1358	76	13	.3	.3	NUM
eurjchem-1358	76	14	.	.	PUNCT
eurjchem-1358	77	1	assay	assay	NOUN
eurjchem-1358	77	2	of	of	ADP
eurjchem-1358	77	3	ob	ob	NOUN
eurjchem-1358	77	4	ba	ba	VERB
eurjchem-1358	77	5	the	the	DET
eurjchem-1358	77	6	procedure	procedure	NOUN
eurjchem-1358	77	7	simultaneous	simultaneous	ADJ
eurjchem-1358	77	8	d	d	NOUN
eurjchem-1358	77	9	pared	pare	VERB
eurjchem-1358	77	10	mixture	mixture	NOUN
eurjchem-1358	77	11	d	d	NOUN
eurjchem-1358	77	12	1.2‐3.5	1.2‐3.5	NUM
eurjchem-1358	77	13	µg	µg	NOUN
eurjchem-1358	77	14	/	/	SYM
eurjchem-1358	77	15	m	m	VERB
eurjchem-1358	77	16	mpleted	mplete	VERB
eurjchem-1358	77	17	to	to	ADP
eurjchem-1358	77	18	the	the	DET
eurjchem-1358	77	19	m	m	NOUN
eurjchem-1358	77	20	ncentrations	ncentration	NOUN
eurjchem-1358	77	21	of	of	ADP
eurjchem-1358	77	22	h	h	NOUN
eurjchem-1358	77	23	from	from	ADP
eurjchem-1358	77	24	its	its	PRON
eurjchem-1358	77	25	calib	calib	NOUN
eurjchem-1358	77	26	ure	ure	NOUN
eurjchem-1358	77	27	2	2	NUM
eurjchem-1358	77	28	.	.	PUNCT
eurjchem-1358	78	1	a	a	DET
eurjchem-1358	78	2	typical	typical	ADJ
eurjchem-1358	78	3	ch	ch	NOUN
eurjchem-1358	78	4	oratory	oratory	NOUN
eurjchem-1358	78	5	prepared	prepare	VERB
eurjchem-1358	78	6	m	m	VERB
eurjchem-1358	78	7	.4	.4	NUM
eurjchem-1358	78	8	.	.	PUNCT
eurjchem-1358	79	1	assay	assay	NOUN
eurjchem-1358	79	2	of	of	ADP
eurjchem-1358	79	3	ob	ob	ADP
eurjchem-1358	79	4	the	the	DET
eurjchem-1358	79	5	sample	sample	NOUN
eurjchem-1358	79	6	so	so	ADV
eurjchem-1358	79	7	uted	uted	ADJ
eurjchem-1358	79	8	,	,	PUNCT
eurjchem-1358	79	9	completed	complete	VERB
eurjchem-1358	79	10	plicates	plicate	NOUN
eurjchem-1358	79	11	(	(	PUNCT
eurjchem-1358	79	12	figur	figur	PROPN
eurjchem-1358	79	13	culated	culate	VERB
eurjchem-1358	79	14	using	use	VERB
eurjchem-1358	79	15	its	its	PRON
eurjchem-1358	79	16	ure	ure	NOUN
eurjchem-1358	79	17	3	3	NUM
eurjchem-1358	79	18	.	.	PUNCT
eurjchem-1358	79	19	a	a	DET
eurjchem-1358	79	20	typical	typical	ADJ
eurjchem-1358	79	21	l	l	PROPN
eurjchem-1358	79	22	ple	ple	PROPN
eurjchem-1358	79	23	.	.	PUNCT
eurjchem-1358	80	1	(	(	PUNCT
eurjchem-1358	80	2	1	1	NUM
eurjchem-1358	80	3	)	)	PUNCT
eurjchem-1358	80	4	(	(	PUNCT
eurjchem-1358	80	5	2016	2016	NUM
eurjchem-1358	80	6	)	)	PUNCT
eurjchem-1358	80	7	97‐10	97‐10	NOUN
eurjchem-1358	81	1	er	er	INTJ
eurjchem-1358	81	2	tablets	tablet	NOUN
eurjchem-1358	81	3	equ	equ	PROPN
eurjchem-1358	81	4	ansferred	ansferre	VERB
eurjchem-1358	81	5	to	to	ADP
eurjchem-1358	81	6	50	50	NUM
eurjchem-1358	81	7	cetonitrile	cetonitrile	ADJ
eurjchem-1358	81	8	wer	wer	NOUN
eurjchem-1358	81	9	min	min	NOUN
eurjchem-1358	81	10	with	with	ADP
eurjchem-1358	81	11	inter	inter	NOUN
eurjchem-1358	81	12	pleted	plete	VERB
eurjchem-1358	81	13	to	to	ADP
eurjchem-1358	81	14	the	the	DET
eurjchem-1358	81	15	ed	ed	NOUN
eurjchem-1358	81	16	discarding	discard	VERB
eurjchem-1358	81	17	fi	fi	NOUN
eurjchem-1358	81	18	e	e	NOUN
eurjchem-1358	81	19	solution	solution	NOUN
eurjchem-1358	81	20	(	(	PUNCT
eurjchem-1358	81	21	1	1	NUM
eurjchem-1358	81	22	mg	mg	NOUN
eurjchem-1358	81	23	on	on	ADP
eurjchem-1358	81	24	of	of	ADP
eurjchem-1358	81	25	calibratio	calibratio	NOUN
eurjchem-1358	81	26	quots	quot	NOUN
eurjchem-1358	81	27	from	from	ADP
eurjchem-1358	81	28	o	o	PROPN
eurjchem-1358	81	29	a	a	DET
eurjchem-1358	81	30	series	series	NOUN
eurjchem-1358	81	31	of	of	ADP
eurjchem-1358	81	32	10	10	NUM
eurjchem-1358	81	33	ompleted	omplete	VERB
eurjchem-1358	81	34	with	with	ADP
eurjchem-1358	81	35	ng	ng	PROPN
eurjchem-1358	81	36	0.5‐100	0.5‐100	NUM
eurjchem-1358	81	37	μg/	μg/	PROPN
eurjchem-1358	81	38	m	m	PROPN
eurjchem-1358	81	39	paba	paba	PROPN
eurjchem-1358	81	40	workin	workin	PROPN
eurjchem-1358	81	41	s	s	PROPN
eurjchem-1358	81	42	of	of	ADP
eurjchem-1358	81	43	10	10	NUM
eurjchem-1358	81	44	ml	ml	PROPN
eurjchem-1358	81	45	volu	volu	PROPN
eurjchem-1358	81	46	mobile	mobile	ADJ
eurjchem-1358	81	47	phase	phase	NOUN
eurjchem-1358	81	48	to	to	ADP
eurjchem-1358	81	49	a	a	DET
eurjchem-1358	81	50	volume	volume	NOUN
eurjchem-1358	81	51	of	of	ADP
eurjchem-1358	81	52	ates	ates	PROPN
eurjchem-1358	81	53	into	into	ADP
eurjchem-1358	81	54	the	the	DET
eurjchem-1358	81	55	ch	ch	NOUN
eurjchem-1358	81	56	obile	obile	NOUN
eurjchem-1358	81	57	phase	phase	NOUN
eurjchem-1358	81	58	at	at	ADP
eurjchem-1358	81	59	nm	nm	PROPN
eurjchem-1358	81	60	were	be	AUX
eurjchem-1358	81	61	adjus	adju	VERB
eurjchem-1358	81	62	tting	tte	VERB
eurjchem-1358	81	63	area	area	NOUN
eurjchem-1358	81	64	und	und	NOUN
eurjchem-1358	81	65	b	b	NOUN
eurjchem-1358	81	66	and	and	CCONJ
eurjchem-1358	81	67	paba	paba	PROPN
eurjchem-1358	81	68	in	in	ADP
eurjchem-1358	81	69	b	b	PROPN
eurjchem-1358	81	70	e	e	NOUN
eurjchem-1358	81	71	mentioned	mention	VERB
eurjchem-1358	81	72	in	in	ADP
eurjchem-1358	81	73	ons	ons	PROPN
eurjchem-1358	81	74	equivalent	equivalent	PROPN
eurjchem-1358	81	75	t	t	PROPN
eurjchem-1358	81	76	in	in	ADP
eurjchem-1358	81	77	bulk	bulk	NOUN
eurjchem-1358	81	78	,	,	PUNCT
eurjchem-1358	81	79	respec	respec	PROPN
eurjchem-1358	81	80	b	b	PROPN
eurjchem-1358	81	81	in	in	ADP
eurjchem-1358	81	82	laboratory	laboratory	NOUN
eurjchem-1358	81	83	e	e	NOUN
eurjchem-1358	81	84	mentioned	mention	VERB
eurjchem-1358	81	85	in	in	ADP
eurjchem-1358	81	86	determination	determination	NOUN
eurjchem-1358	81	87	o	o	X
eurjchem-1358	81	88	s	s	AUX
eurjchem-1358	81	89	using	use	VERB
eurjchem-1358	81	90	concen	concen	NOUN
eurjchem-1358	81	91	ml	ml	PROPN
eurjchem-1358	81	92	of	of	ADP
eurjchem-1358	81	93	ob	ob	ADP
eurjchem-1358	81	94	an	an	DET
eurjchem-1358	81	95	mark	mark	NOUN
eurjchem-1358	81	96	by	by	ADP
eurjchem-1358	81	97	mobile	mobile	ADJ
eurjchem-1358	81	98	f	f	PROPN
eurjchem-1358	81	99	ob	ob	ADJ
eurjchem-1358	81	100	and	and	CCONJ
eurjchem-1358	81	101	paba	paba	NOUN
eurjchem-1358	81	102	ration	ration	NOUN
eurjchem-1358	81	103	equation	equation	NOUN
eurjchem-1358	81	104	hromatogram	hromatogram	NOUN
eurjchem-1358	81	105	of	of	ADP
eurjchem-1358	81	106	75	75	NUM
eurjchem-1358	81	107	mixture	mixture	NOUN
eurjchem-1358	81	108	.	.	PUNCT
eurjchem-1358	82	1	b	b	NOUN
eurjchem-1358	82	2	in	in	ADP
eurjchem-1358	82	3	pharmaceu	pharmaceu	NOUN
eurjchem-1358	82	4	olution	olution	NOUN
eurjchem-1358	82	5	prepare	prepare	VERB
eurjchem-1358	82	6	d	d	NOUN
eurjchem-1358	82	7	with	with	ADP
eurjchem-1358	82	8	mobile	mobile	NOUN
eurjchem-1358	82	9	re	re	NOUN
eurjchem-1358	82	10	3	3	NUM
eurjchem-1358	82	11	)	)	PUNCT
eurjchem-1358	82	12	.	.	PUNCT
eurjchem-1358	83	1	the	the	DET
eurjchem-1358	83	2	c	c	PROPN
eurjchem-1358	83	3	s	s	PROPN
eurjchem-1358	83	4	calibration	calibration	NOUN
eurjchem-1358	83	5	eq	eq	ADP
eurjchem-1358	83	6	c	c	PROPN
eurjchem-1358	83	7	chromatogram	chromatogram	PROPN
eurjchem-1358	83	8	01	01	NUM
eurjchem-1358	83	9	uivalent	uivalent	NOUN
eurjchem-1358	83	10	to	to	ADP
eurjchem-1358	83	11	50	50	NUM
eurjchem-1358	83	12	ml	ml	NOUN
eurjchem-1358	83	13	volumetric	volumetric	NOUN
eurjchem-1358	83	14	re	re	VERB
eurjchem-1358	83	15	added	add	VERB
eurjchem-1358	83	16	.	.	PUNCT
eurjchem-1358	84	1	the	the	DET
eurjchem-1358	84	2	rmediate	rmediate	NOUN
eurjchem-1358	84	3	shakin	shakin	PROPN
eurjchem-1358	84	4	mark	mark	VERB
eurjchem-1358	84	5	with	with	ADP
eurjchem-1358	84	6	ac	ac	PROPN
eurjchem-1358	84	7	irst	irst	ADV
eurjchem-1358	84	8	10	10	NUM
eurjchem-1358	84	9	ml	ml	NOUN
eurjchem-1358	84	10	and	and	CCONJ
eurjchem-1358	84	11	g	g	NOUN
eurjchem-1358	84	12	/	/	SYM
eurjchem-1358	84	13	ml	ml	NOUN
eurjchem-1358	84	14	)	)	PUNCT
eurjchem-1358	84	15	.	.	PUNCT
eurjchem-1358	85	1	n	n	ADP
eurjchem-1358	85	2	curves	curve	NOUN
eurjchem-1358	85	3	ob	ob	VERB
eurjchem-1358	85	4	working	work	VERB
eurjchem-1358	85	5	s	s	PROPN
eurjchem-1358	85	6	0	0	NUM
eurjchem-1358	85	7	ml	ml	NOUN
eurjchem-1358	85	8	volumet	volumet	NOUN
eurjchem-1358	85	9	h	h	PROPN
eurjchem-1358	85	10	the	the	DET
eurjchem-1358	85	11	mobile	mobile	NOUN
eurjchem-1358	85	12	/ml	/ml	PUNCT
eurjchem-1358	85	13	ob	ob	PROPN
eurjchem-1358	85	14	.	.	PROPN
eurjchem-1358	85	15	altern	altern	PROPN
eurjchem-1358	85	16	ng	ng	PROPN
eurjchem-1358	85	17	solution	solution	NOUN
eurjchem-1358	85	18	we	we	PRON
eurjchem-1358	85	19	umetric	umetric	ADJ
eurjchem-1358	85	20	flasks	flask	NOUN
eurjchem-1358	85	21	,	,	PUNCT
eurjchem-1358	85	22	o	o	NOUN
eurjchem-1358	85	23	give	give	VERB
eurjchem-1358	85	24	solutions	solution	NOUN
eurjchem-1358	85	25	2	2	NUM
eurjchem-1358	85	26	µl	µl	ADP
eurjchem-1358	85	27	of	of	ADP
eurjchem-1358	85	28	each	each	DET
eurjchem-1358	85	29	hromatograph	hromatograph	NOUN
eurjchem-1358	85	30	.	.	PUNCT
eurjchem-1358	86	1	flow	flow	NOUN
eurjchem-1358	86	2	rate	rate	NOUN
eurjchem-1358	86	3	0.8	0.8	NUM
eurjchem-1358	86	4	sted	ste	VERB
eurjchem-1358	86	5	.	.	PUNCT
eurjchem-1358	87	1	calibratio	calibratio	PROPN
eurjchem-1358	87	2	der	der	NOUN
eurjchem-1358	87	3	the	the	DET
eurjchem-1358	87	4	peak	peak	NOUN
eurjchem-1358	87	5	bulk	bulk	NOUN
eurjchem-1358	87	6	n	n	NOUN
eurjchem-1358	87	7	section	section	NOUN
eurjchem-1358	87	8	2.6.1	2.6.1	NUM
eurjchem-1358	87	9	to	to	ADP
eurjchem-1358	87	10	3‐70	3‐70	NUM
eurjchem-1358	87	11	μg	μg	NOUN
eurjchem-1358	87	12	/	/	SYM
eurjchem-1358	87	13	ml	ml	X
eurjchem-1358	87	14	tively	tively	ADV
eurjchem-1358	87	15	.	.	PUNCT
eurjchem-1358	88	1	prepared	prepare	VERB
eurjchem-1358	88	2	mixt	mixt	ADJ
eurjchem-1358	88	3	n	n	PRON
eurjchem-1358	88	4	section	section	NOUN
eurjchem-1358	88	5	2.6.1	2.6.1	NUM
eurjchem-1358	88	6	of	of	ADP
eurjchem-1358	88	7	ob	ob	NOUN
eurjchem-1358	88	8	and	and	CCONJ
eurjchem-1358	88	9	paba	paba	PROPN
eurjchem-1358	88	10	ntrations	ntration	NOUN
eurjchem-1358	88	11	equiv	equiv	PROPN
eurjchem-1358	88	12	nd	nd	PRON
eurjchem-1358	88	13	paba	paba	PROPN
eurjchem-1358	88	14	,	,	PUNCT
eurjchem-1358	88	15	res	re	NOUN
eurjchem-1358	88	16	e	e	NOUN
eurjchem-1358	88	17	phase	phase	NOUN
eurjchem-1358	88	18	(	(	PUNCT
eurjchem-1358	88	19	figure	figure	VERB
eurjchem-1358	88	20	a	a	PRON
eurjchem-1358	88	21	were	be	AUX
eurjchem-1358	88	22	separa	separa	PROPN
eurjchem-1358	88	23	n.	n.	PROPN
eurjchem-1358	88	24	5	5	NUM
eurjchem-1358	88	25	µg	µg	NOUN
eurjchem-1358	88	26	/	/	SYM
eurjchem-1358	88	27	ml	ml	NOUN
eurjchem-1358	88	28	ob	ob	NOUN
eurjchem-1358	88	29	and	and	CCONJ
eurjchem-1358	88	30	1	1	NUM
eurjchem-1358	88	31	utical	utical	ADJ
eurjchem-1358	88	32	preparat	preparat	PROPN
eurjchem-1358	88	33	ed	ed	NOUN
eurjchem-1358	88	34	in	in	ADP
eurjchem-1358	88	35	section	section	NOUN
eurjchem-1358	88	36	2	2	NUM
eurjchem-1358	88	37	phase	phase	NOUN
eurjchem-1358	88	38	and	and	CCONJ
eurjchem-1358	88	39	th	th	X
eurjchem-1358	88	40	oncentrations	oncentration	NOUN
eurjchem-1358	88	41	quation	quation	NOUN
eurjchem-1358	88	42	.	.	PUNCT
eurjchem-1358	89	1	of	of	ADP
eurjchem-1358	89	2	50	50	NUM
eurjchem-1358	89	3	µg	µg	NOUN
eurjchem-1358	89	4	/	/	SYM
eurjchem-1358	89	5	ml	ml	NOUN
eurjchem-1358	89	6	of	of	ADP
eurjchem-1358	89	7	o	o	PROPN
eurjchem-1358	89	8	mg	mg	PROPN
eurjchem-1358	89	9	otilonium	otilonium	PROPN
eurjchem-1358	89	10	c	c	VERB
eurjchem-1358	89	11	flask	flask	NOUN
eurjchem-1358	89	12	to	to	PART
eurjchem-1358	89	13	which	which	DET
eurjchem-1358	89	14	solution	solution	NOUN
eurjchem-1358	89	15	was	be	AUX
eurjchem-1358	89	16	ng	ng	PROPN
eurjchem-1358	89	17	.	.	PUNCT
eurjchem-1358	90	1	finally	finally	ADV
eurjchem-1358	90	2	,	,	PUNCT
eurjchem-1358	90	3	the	the	DET
eurjchem-1358	90	4	cetonitrile	cetonitrile	NOUN
eurjchem-1358	90	5	.	.	PUNCT
eurjchem-1358	91	1	the	the	DET
eurjchem-1358	91	2	the	the	DET
eurjchem-1358	91	3	filtrate	filtrate	NOUN
eurjchem-1358	91	4	was	be	AUX
eurjchem-1358	91	5	solution	solution	NOUN
eurjchem-1358	91	6	were	be	AUX
eurjchem-1358	91	7	tric	tric	ADJ
eurjchem-1358	91	8	flasks	flask	NOUN
eurjchem-1358	91	9	,	,	PUNCT
eurjchem-1358	91	10	the	the	DET
eurjchem-1358	91	11	phase	phase	NOUN
eurjchem-1358	91	12	to	to	PART
eurjchem-1358	91	13	give	give	VERB
eurjchem-1358	91	14	natively	natively	ADV
eurjchem-1358	91	15	,	,	PUNCT
eurjchem-1358	91	16	differ‐	differ‐	PROPN
eurjchem-1358	91	17	ere	ere	PROPN
eurjchem-1358	91	18	transferred	transfer	VERB
eurjchem-1358	91	19	and	and	CCONJ
eurjchem-1358	91	20	completed	complete	VERB
eurjchem-1358	91	21	s	s	PRON
eurjchem-1358	91	22	containing	contain	VERB
eurjchem-1358	91	23	1‐	1‐	NUM
eurjchem-1358	91	24	h	h	NOUN
eurjchem-1358	91	25	solution	solution	NOUN
eurjchem-1358	91	26	was	be	AUX
eurjchem-1358	91	27	the	the	DET
eurjchem-1358	91	28	conditions	condition	NOUN
eurjchem-1358	91	29	8	8	NUM
eurjchem-1358	91	30	ml	ml	NOUN
eurjchem-1358	91	31	/	/	SYM
eurjchem-1358	91	32	min	min	NOUN
eurjchem-1358	91	33	and	and	CCONJ
eurjchem-1358	91	34	on	on	ADP
eurjchem-1358	91	35	curves	curve	NOUN
eurjchem-1358	91	36	were	be	AUX
eurjchem-1358	91	37	(	(	PUNCT
eurjchem-1358	91	38	aup	aup	PROPN
eurjchem-1358	91	39	)	)	PUNCT
eurjchem-1358	91	40	against	against	ADP
eurjchem-1358	91	41	1	1	NUM
eurjchem-1358	91	42	was	be	AUX
eurjchem-1358	91	43	repeated	repeat	VERB
eurjchem-1358	91	44	ob	ob	ADP
eurjchem-1358	91	45	in	in	ADP
eurjchem-1358	91	46	bulk	bulk	NOUN
eurjchem-1358	91	47	and	and	CCONJ
eurjchem-1358	91	48	tures	ture	NOUN
eurjchem-1358	91	49	with	with	ADP
eurjchem-1358	91	50	1	1	NUM
eurjchem-1358	91	51	was	be	AUX
eurjchem-1358	91	52	repeated	repeat	VERB
eurjchem-1358	91	53	a	a	PRON
eurjchem-1358	91	54	in	in	ADP
eurjchem-1358	91	55	laboratory	laboratory	NOUN
eurjchem-1358	91	56	valent	valent	NOUN
eurjchem-1358	91	57	to	to	ADP
eurjchem-1358	91	58	10‐96	10‐96	NUM
eurjchem-1358	91	59	pectively	pectively	ADV
eurjchem-1358	91	60	,	,	PUNCT
eurjchem-1358	91	61	and	and	CCONJ
eurjchem-1358	91	62	e	e	NOUN
eurjchem-1358	91	63	2	2	NUM
eurjchem-1358	91	64	)	)	PUNCT
eurjchem-1358	91	65	.	.	PUNCT
eurjchem-1358	92	1	recovered	recover	VERB
eurjchem-1358	92	2	ately	ately	ADV
eurjchem-1358	92	3	calculated	calculate	VERB
eurjchem-1358	92	4	1.5	1.5	NUM
eurjchem-1358	92	5	µg	µg	NOUN
eurjchem-1358	92	6	/	/	SYM
eurjchem-1358	92	7	ml	ml	NOUN
eurjchem-1358	92	8	paba	paba	NOUN
eurjchem-1358	92	9	in	in	ADP
eurjchem-1358	92	10	tions	tion	NOUN
eurjchem-1358	92	11	2.5	2.5	NUM
eurjchem-1358	92	12	was	be	AUX
eurjchem-1358	92	13	serially	serially	ADV
eurjchem-1358	92	14	hen	hen	NOUN
eurjchem-1358	92	15	injected	inject	VERB
eurjchem-1358	92	16	in	in	ADP
eurjchem-1358	92	17	of	of	ADP
eurjchem-1358	92	18	ob	ob	NOUN
eurjchem-1358	92	19	were	be	AUX
eurjchem-1358	92	20	otilonium	otilonium	NOUN
eurjchem-1358	92	21	bromide	bromide	NOUN
eurjchem-1358	92	22	m	m	NOUN
eurjchem-1358	93	1	h	h	NOUN
eurjchem-1358	93	2	s	s	PART
eurjchem-1358	93	3	e	e	X
eurjchem-1358	93	4	e	e	NOUN
eurjchem-1358	93	5	s	s	X
eurjchem-1358	93	6	e	e	X
eurjchem-1358	93	7	e	e	X
eurjchem-1358	93	8	e	e	X
eurjchem-1358	93	9	‐	‐	PROPN
eurjchem-1358	93	10	d	d	PROPN
eurjchem-1358	93	11	d	d	PROPN
eurjchem-1358	93	12	‐	‐	ADP
eurjchem-1358	93	13	s	s	PART
eurjchem-1358	93	14	s	s	X
eurjchem-1358	93	15	d	d	X
eurjchem-1358	93	16	e	e	NOUN
eurjchem-1358	93	17	t	t	PROPN
eurjchem-1358	93	18	d	d	X
eurjchem-1358	93	19	d	d	PROPN
eurjchem-1358	94	1	d	d	X
eurjchem-1358	94	2	y	y	PROPN
eurjchem-1358	94	3	6	6	NUM
eurjchem-1358	94	4	d	d	NOUN
eurjchem-1358	94	5	d	d	PROPN
eurjchem-1358	94	6	d	d	PROPN
eurjchem-1358	94	7	n	n	PROPN
eurjchem-1358	94	8	y	y	PROPN
eurjchem-1358	94	9	n	n	ADV
eurjchem-1358	94	10	e	e	X
eurjchem-1358	94	11	e	e	X
eurjchem-1358	94	12	el‐kerdawy	el‐kerdawy	PROPN
eurjchem-1358	94	13	et	et	PROPN
eurjchem-1358	94	14	al	al	PROPN
eurjchem-1358	94	15	.	.	PUNCT
eurjchem-1358	94	16	/	/	SYM
eurjchem-1358	94	17	european	european	PROPN
eurjchem-1358	94	18	journal	journal	PROPN
eurjchem-1358	94	19	of	of	ADP
eurjchem-1358	94	20	chemistry	chemistry	NOUN
eurjchem-1358	94	21	7	7	NUM
eurjchem-1358	94	22	(	(	PUNCT
eurjchem-1358	94	23	1	1	NUM
eurjchem-1358	94	24	)	)	PUNCT
eurjchem-1358	94	25	(	(	PUNCT
eurjchem-1358	94	26	2016	2016	NUM
eurjchem-1358	94	27	)	)	PUNCT
eurjchem-1358	94	28	97‐101	97‐101	PROPN
eurjchem-1358	94	29	99	99	NUM
eurjchem-1358	94	30	table	table	NOUN
eurjchem-1358	94	31	1	1	NUM
eurjchem-1358	94	32	.	.	PUNCT
eurjchem-1358	94	33	system	system	NOUN
eurjchem-1358	94	34	suitability	suitability	NOUN
eurjchem-1358	94	35	tests	test	VERB
eurjchem-1358	94	36	for	for	ADP
eurjchem-1358	94	37	the	the	DET
eurjchem-1358	94	38	proposed	propose	VERB
eurjchem-1358	94	39	lc	lc	NOUN
eurjchem-1358	94	40	method	method	NOUN
eurjchem-1358	94	41	.	.	PUNCT
eurjchem-1358	95	1	data	datum	NOUN
eurjchem-1358	95	2	for	for	ADP
eurjchem-1358	95	3	paba	paba	PROPN
eurjchem-1358	95	4	data	datum	NOUN
eurjchem-1358	95	5	for	for	ADP
eurjchem-1358	95	6	ob	ob	NOUN
eurjchem-1358	95	7	item	item	NOUN
eurjchem-1358	95	8	6674	6674	NUM
eurjchem-1358	95	9	6320n	6320n	NUM
eurjchem-1358	95	10	,	,	PUNCT
eurjchem-1358	95	11	no	no	PRON
eurjchem-1358	95	12	of	of	ADP
eurjchem-1358	95	13	theoretical	theoretical	ADJ
eurjchem-1358	95	14	plates	plate	NOUN
eurjchem-1358	95	15	per	per	ADP
eurjchem-1358	95	16	column	column	NOUN
eurjchem-1358	95	17	1.07	1.07	NUM
eurjchem-1358	95	18	1.16	1.16	NUM
eurjchem-1358	95	19	t	t	NOUN
eurjchem-1358	95	20	,	,	PUNCT
eurjchem-1358	95	21	tailing	tail	VERB
eurjchem-1358	95	22	factor	factor	NOUN
eurjchem-1358	95	23	0.101	0.101	NUM
eurjchem-1358	95	24	0.170%r.s.d	0.170%r.s.d	NUM
eurjchem-1358	95	25	.	.	PUNCT
eurjchem-1358	96	1	of	of	ADP
eurjchem-1358	96	2	six	six	NUM
eurjchem-1358	96	3	injections	injection	NOUN
eurjchem-1358	96	4	peak	peak	NOUN
eurjchem-1358	96	5	area	area	NOUN
eurjchem-1358	96	6	0.08	0.08	NUM
eurjchem-1358	96	7	0.25	0.25	NUM
eurjchem-1358	96	8	%	%	NOUN
eurjchem-1358	96	9	r.s.d	r.s.d	NOUN
eurjchem-1358	96	10	of	of	ADP
eurjchem-1358	96	11	six	six	NUM
eurjchem-1358	96	12	injection	injection	NOUN
eurjchem-1358	96	13	of	of	ADP
eurjchem-1358	96	14	retention	retention	NOUN
eurjchem-1358	96	15	time	time	NOUN
eurjchem-1358	96	16	(	(	PUNCT
eurjchem-1358	96	17	min	min	NOUN
eurjchem-1358	96	18	)	)	PUNCT
eurjchem-1358	96	19	14.63	14.63	NUM
eurjchem-1358	96	20	14.63r	14.63r	NUM
eurjchem-1358	96	21	,	,	PUNCT
eurjchem-1358	96	22	resolution	resolution	NOUN
eurjchem-1358	96	23	factor	factor	NOUN
eurjchem-1358	96	24	%	%	NOUN
eurjchem-1358	96	25	r.s.d	r.s.d	NOUN
eurjchem-1358	96	26	:	:	PUNCT
eurjchem-1358	96	27	%	%	NOUN
eurjchem-1358	96	28	relative	relative	ADJ
eurjchem-1358	96	29	standard	standard	ADJ
eurjchem-1358	96	30	deviation	deviation	NOUN
eurjchem-1358	96	31	.	.	PUNCT
eurjchem-1358	97	1	table	table	NOUN
eurjchem-1358	97	2	2	2	NUM
eurjchem-1358	97	3	.	.	PUNCT
eurjchem-1358	98	1	results	result	NOUN
eurjchem-1358	98	2	obtained	obtain	VERB
eurjchem-1358	98	3	by	by	ADP
eurjchem-1358	98	4	the	the	DET
eurjchem-1358	98	5	proposed	propose	VERB
eurjchem-1358	98	6	lc	lc	NOUN
eurjchem-1358	98	7	method	method	NOUN
eurjchem-1358	98	8	for	for	ADP
eurjchem-1358	98	9	the	the	DET
eurjchem-1358	98	10	determination	determination	NOUN
eurjchem-1358	98	11	of	of	ADP
eurjchem-1358	98	12	ob	ob	NOUN
eurjchem-1358	98	13	and	and	CCONJ
eurjchem-1358	98	14	paba	paba	PROPN
eurjchem-1358	98	15	.	.	PUNCT
eurjchem-1358	99	1	item	item	PROPN
eurjchem-1358	99	2	ob	ob	ADP
eurjchem-1358	99	3	paba	paba	PROPN
eurjchem-1358	99	4	retention	retention	NOUN
eurjchem-1358	99	5	time	time	NOUN
eurjchem-1358	99	6	4.97±0.012	4.97±0.012	PROPN
eurjchem-1358	99	7	2.03±0.002	2.03±0.002	NUM
eurjchem-1358	99	8	wavelength	wavelength	NOUN
eurjchem-1358	99	9	of	of	ADP
eurjchem-1358	99	10	detection	detection	NOUN
eurjchem-1358	99	11	,	,	PUNCT
eurjchem-1358	99	12	nm	nm	PROPN
eurjchem-1358	99	13	290	290	NUM
eurjchem-1358	99	14	290	290	NUM
eurjchem-1358	99	15	linearity	linearity	NOUN
eurjchem-1358	99	16	range	range	NOUN
eurjchem-1358	99	17	,	,	PUNCT
eurjchem-1358	99	18	µg	µg	ADJ
eurjchem-1358	99	19	/	/	SYM
eurjchem-1358	99	20	ml	ml	NOUN
eurjchem-1358	99	21	0.5‐100	0.5‐100	NUM
eurjchem-1358	99	22	1‐50	1‐50	NUM
eurjchem-1358	99	23	regression	regression	NOUN
eurjchem-1358	99	24	equation	equation	NOUN
eurjchem-1358	99	25	y	y	NOUN
eurjchem-1358	99	26	=	=	PUNCT
eurjchem-1358	99	27	7.0898	7.0898	NUM
eurjchem-1358	99	28	x	x	SYM
eurjchem-1358	99	29	‐	‐	ADP
eurjchem-1358	99	30	1.2818	1.2818	NUM
eurjchem-1358	99	31	y	y	NOUN
eurjchem-1358	99	32	=	=	SYM
eurjchem-1358	99	33	18.591	18.591	NUM
eurjchem-1358	99	34	x	x	SYM
eurjchem-1358	99	35	‐	‐	ADP
eurjchem-1358	99	36	0.4337	0.4337	NUM
eurjchem-1358	99	37	regression	regression	NOUN
eurjchem-1358	99	38	coefficient	coefficient	NOUN
eurjchem-1358	99	39	(	(	PUNCT
eurjchem-1358	99	40	r2	r2	PROPN
eurjchem-1358	99	41	)	)	PUNCT
eurjchem-1358	99	42	1.000	1.000	NUM
eurjchem-1358	99	43	0.9998	0.9998	NUM
eurjchem-1358	99	44	sa	sa	NOUN
eurjchem-1358	99	45	,	,	PUNCT
eurjchem-1358	99	46	standard	standard	ADJ
eurjchem-1358	99	47	deviation	deviation	NOUN
eurjchem-1358	99	48	of	of	ADP
eurjchem-1358	99	49	intercept	intercept	NOUN
eurjchem-1358	99	50	1.0000	1.0000	NUM
eurjchem-1358	99	51	3.8277	3.8277	NUM
eurjchem-1358	99	52	sb	sb	NOUN
eurjchem-1358	99	53	,	,	PUNCT
eurjchem-1358	99	54	standard	standard	ADJ
eurjchem-1358	99	55	deviation	deviation	NOUN
eurjchem-1358	99	56	of	of	ADP
eurjchem-1358	99	57	slope	slope	NOUN
eurjchem-1358	99	58	0.0200	0.0200	NUM
eurjchem-1358	99	59	0.1264	0.1264	NUM
eurjchem-1358	99	60	confidence	confidence	NOUN
eurjchem-1358	99	61	limit	limit	NOUN
eurjchem-1358	99	62	for	for	ADP
eurjchem-1358	99	63	the	the	DET
eurjchem-1358	99	64	slope	slope	NOUN
eurjchem-1358	99	65	7.0898±0.0541	7.0898±0.0541	NUM
eurjchem-1358	99	66	18.548±0.3514	18.548±0.3514	NUM
eurjchem-1358	99	67	confidence	confidence	NOUN
eurjchem-1358	99	68	limit	limit	NOUN
eurjchem-1358	99	69	for	for	ADP
eurjchem-1358	99	70	the	the	DET
eurjchem-1358	99	71	intercept	intercept	NOUN
eurjchem-1358	99	72	‐1.2817±2.821	‐1.2817±2.821	PROPN
eurjchem-1358	99	73	‐0.4337±10.65	‐0.4337±10.65	NOUN
eurjchem-1358	99	74	limit	limit	NOUN
eurjchem-1358	99	75	of	of	ADP
eurjchem-1358	99	76	quantification	quantification	NOUN
eurjchem-1358	99	77	,	,	PUNCT
eurjchem-1358	99	78	loq	loq	PROPN
eurjchem-1358	99	79	,	,	PUNCT
eurjchem-1358	99	80	μg	μg	PROPN
eurjchem-1358	99	81	/	/	SYM
eurjchem-1358	99	82	ml	ml	PROPN
eurjchem-1358	99	83	0.2018	0.2018	NUM
eurjchem-1358	99	84	0.5980	0.5980	NUM
eurjchem-1358	99	85	limit	limit	NOUN
eurjchem-1358	99	86	of	of	ADP
eurjchem-1358	99	87	detection	detection	NOUN
eurjchem-1358	99	88	,	,	PUNCT
eurjchem-1358	99	89	lod	lod	PROPN
eurjchem-1358	99	90	,	,	PUNCT
eurjchem-1358	99	91	μg	μg	PROPN
eurjchem-1358	99	92	/	/	SYM
eurjchem-1358	99	93	ml	ml	VERB
eurjchem-1358	99	94	0.0665	0.0665	NUM
eurjchem-1358	99	95	0.1974	0.1974	NUM
eurjchem-1358	99	96	drug	drug	NOUN
eurjchem-1358	99	97	in	in	ADP
eurjchem-1358	99	98	bulk	bulk	ADJ
eurjchem-1358	99	99	100.31±2.142	100.31±2.142	NUM
eurjchem-1358	99	100	99.96±1.615	99.96±1.615	NUM
eurjchem-1358	99	101	recovery	recovery	NOUN
eurjchem-1358	99	102	for	for	ADP
eurjchem-1358	99	103	standard	standard	ADJ
eurjchem-1358	99	104	added	add	VERB
eurjchem-1358	99	105	100.07±0.422	100.07±0.422	NOUN
eurjchem-1358	99	106	‐	‐	NOUN
eurjchem-1358	99	107	recovery	recovery	NOUN
eurjchem-1358	99	108	for	for	ADP
eurjchem-1358	99	109	drug	drug	NOUN
eurjchem-1358	99	110	in	in	ADP
eurjchem-1358	99	111	laboratory	laboratory	NOUN
eurjchem-1358	99	112	prepared	prepare	VERB
eurjchem-1358	99	113	mixtures	mixture	NOUN
eurjchem-1358	99	114	101.35±0.759	101.35±0.759	PRON
eurjchem-1358	99	115	101.57±0.816	101.57±0.816	NUM
eurjchem-1358	99	116	3	3	NUM
eurjchem-1358	99	117	.	.	NOUN
eurjchem-1358	99	118	results	result	NOUN
eurjchem-1358	99	119	and	and	CCONJ
eurjchem-1358	99	120	discussion	discussion	NOUN
eurjchem-1358	99	121	3.1	3.1	NUM
eurjchem-1358	99	122	.	.	PUNCT
eurjchem-1358	100	1	method	method	PROPN
eurjchem-1358	100	2	development	development	NOUN
eurjchem-1358	100	3	the	the	DET
eurjchem-1358	100	4	core	core	NOUN
eurjchem-1358	100	5	intention	intention	NOUN
eurjchem-1358	100	6	of	of	ADP
eurjchem-1358	100	7	this	this	DET
eurjchem-1358	100	8	paper	paper	NOUN
eurjchem-1358	100	9	was	be	AUX
eurjchem-1358	100	10	to	to	PART
eurjchem-1358	100	11	develop	develop	VERB
eurjchem-1358	100	12	a	a	DET
eurjchem-1358	100	13	stability	stability	NOUN
eurjchem-1358	100	14	indicating	indicate	VERB
eurjchem-1358	100	15	assay	assay	VERB
eurjchem-1358	100	16	for	for	ADP
eurjchem-1358	100	17	ob	ob	NOUN
eurjchem-1358	100	18	with	with	ADP
eurjchem-1358	100	19	a	a	DET
eurjchem-1358	100	20	short	short	ADJ
eurjchem-1358	100	21	run	run	NOUN
eurjchem-1358	100	22	time	time	NOUN
eurjchem-1358	100	23	to	to	PART
eurjchem-1358	100	24	allow	allow	VERB
eurjchem-1358	100	25	for	for	ADP
eurjchem-1358	100	26	the	the	DET
eurjchem-1358	100	27	high	high	ADJ
eurjchem-1358	100	28	capacity	capacity	NOUN
eurjchem-1358	100	29	of	of	ADP
eurjchem-1358	100	30	quality	quality	NOUN
eurjchem-1358	100	31	control	control	NOUN
eurjchem-1358	100	32	laboratories	laboratory	NOUN
eurjchem-1358	100	33	.	.	PUNCT
eurjchem-1358	101	1	thus	thus	ADV
eurjchem-1358	101	2	,	,	PUNCT
eurjchem-1358	101	3	the	the	DET
eurjchem-1358	101	4	conditions	condition	NOUN
eurjchem-1358	101	5	affecting	affect	VERB
eurjchem-1358	101	6	the	the	DET
eurjchem-1358	101	7	chromatographic	chromatographic	ADJ
eurjchem-1358	101	8	performance	performance	NOUN
eurjchem-1358	101	9	were	be	AUX
eurjchem-1358	101	10	carefully	carefully	ADV
eurjchem-1358	101	11	studied	study	VERB
eurjchem-1358	101	12	in	in	ADP
eurjchem-1358	101	13	order	order	NOUN
eurjchem-1358	101	14	to	to	PART
eurjchem-1358	101	15	recognize	recognize	VERB
eurjchem-1358	101	16	the	the	DET
eurjchem-1358	101	17	most	most	ADV
eurjchem-1358	101	18	suitable	suitable	ADJ
eurjchem-1358	101	19	chromatographic	chromatographic	ADJ
eurjchem-1358	101	20	system	system	NOUN
eurjchem-1358	101	21	for	for	ADP
eurjchem-1358	101	22	determination	determination	NOUN
eurjchem-1358	101	23	of	of	ADP
eurjchem-1358	101	24	ob	ob	NOUN
eurjchem-1358	101	25	in	in	ADP
eurjchem-1358	101	26	presence	presence	NOUN
eurjchem-1358	101	27	of	of	ADP
eurjchem-1358	101	28	its	its	PRON
eurjchem-1358	101	29	degradation	degradation	NOUN
eurjchem-1358	101	30	product	product	NOUN
eurjchem-1358	101	31	,	,	PUNCT
eurjchem-1358	101	32	paba	paba	PROPN
eurjchem-1358	101	33	.	.	PUNCT
eurjchem-1358	102	1	the	the	DET
eurjchem-1358	102	2	choice	choice	NOUN
eurjchem-1358	102	3	was	be	AUX
eurjchem-1358	102	4	based	base	VERB
eurjchem-1358	102	5	on	on	ADP
eurjchem-1358	102	6	the	the	DET
eurjchem-1358	102	7	highest	high	ADJ
eurjchem-1358	102	8	number	number	NOUN
eurjchem-1358	102	9	of	of	ADP
eurjchem-1358	102	10	theoretical	theoretical	ADJ
eurjchem-1358	102	11	plates	plate	NOUN
eurjchem-1358	102	12	and	and	CCONJ
eurjchem-1358	102	13	the	the	DET
eurjchem-1358	102	14	best	good	ADJ
eurjchem-1358	102	15	resolution	resolution	NOUN
eurjchem-1358	102	16	between	between	ADP
eurjchem-1358	102	17	the	the	DET
eurjchem-1358	102	18	two	two	NUM
eurjchem-1358	102	19	peaks	peak	NOUN
eurjchem-1358	102	20	.	.	PUNCT
eurjchem-1358	103	1	the	the	DET
eurjchem-1358	103	2	selection	selection	NOUN
eurjchem-1358	103	3	of	of	ADP
eurjchem-1358	103	4	the	the	DET
eurjchem-1358	103	5	mobile	mobile	ADJ
eurjchem-1358	103	6	phase	phase	NOUN
eurjchem-1358	103	7	is	be	AUX
eurjchem-1358	103	8	of	of	ADP
eurjchem-1358	103	9	prime	prime	ADJ
eurjchem-1358	103	10	importance	importance	NOUN
eurjchem-1358	103	11	in	in	ADP
eurjchem-1358	103	12	the	the	DET
eurjchem-1358	103	13	development	development	NOUN
eurjchem-1358	103	14	of	of	ADP
eurjchem-1358	103	15	a	a	DET
eurjchem-1358	103	16	chromatographic	chromatographic	ADJ
eurjchem-1358	103	17	technique	technique	NOUN
eurjchem-1358	103	18	for	for	ADP
eurjchem-1358	103	19	proper	proper	ADJ
eurjchem-1358	103	20	elution	elution	NOUN
eurjchem-1358	103	21	,	,	PUNCT
eurjchem-1358	103	22	resolution	resolution	NOUN
eurjchem-1358	103	23	,	,	PUNCT
eurjchem-1358	103	24	symmetrical	symmetrical	ADJ
eurjchem-1358	103	25	peak	peak	NOUN
eurjchem-1358	103	26	shapes	shape	NOUN
eurjchem-1358	103	27	and	and	CCONJ
eurjchem-1358	103	28	reproducibility	reproducibility	NOUN
eurjchem-1358	103	29	of	of	ADP
eurjchem-1358	103	30	the	the	DET
eurjchem-1358	103	31	analytes	analyte	NOUN
eurjchem-1358	103	32	[	[	X
eurjchem-1358	103	33	20	20	NUM
eurjchem-1358	103	34	]	]	PUNCT
eurjchem-1358	103	35	.	.	PUNCT
eurjchem-1358	104	1	several	several	ADJ
eurjchem-1358	104	2	mobile	mobile	ADJ
eurjchem-1358	104	3	phases	phase	NOUN
eurjchem-1358	104	4	were	be	AUX
eurjchem-1358	104	5	evaluated	evaluate	VERB
eurjchem-1358	104	6	using	use	VERB
eurjchem-1358	104	7	various	various	ADJ
eurjchem-1358	104	8	proportions	proportion	NOUN
eurjchem-1358	104	9	of	of	ADP
eurjchem-1358	104	10	different	different	ADJ
eurjchem-1358	104	11	aqueous	aqueous	ADJ
eurjchem-1358	104	12	phases	phase	NOUN
eurjchem-1358	104	13	and	and	CCONJ
eurjchem-1358	104	14	organic	organic	ADJ
eurjchem-1358	104	15	modifiers	modifier	NOUN
eurjchem-1358	104	16	.	.	PUNCT
eurjchem-1358	105	1	methanol	methanol	NOUN
eurjchem-1358	105	2	was	be	AUX
eurjchem-1358	105	3	tried	try	VERB
eurjchem-1358	105	4	as	as	ADP
eurjchem-1358	105	5	organic	organic	ADJ
eurjchem-1358	105	6	modifier	modifier	NOUN
eurjchem-1358	105	7	;	;	PUNCT
eurjchem-1358	105	8	broad	broad	ADJ
eurjchem-1358	105	9	peaks	peak	NOUN
eurjchem-1358	105	10	with	with	ADP
eurjchem-1358	105	11	insufficient	insufficient	ADJ
eurjchem-1358	105	12	separation	separation	NOUN
eurjchem-1358	105	13	were	be	AUX
eurjchem-1358	105	14	obtained	obtain	VERB
eurjchem-1358	105	15	.	.	PUNCT
eurjchem-1358	106	1	triethylamine	triethylamine	NOUN
eurjchem-1358	106	2	and	and	CCONJ
eurjchem-1358	106	3	1‐octane	1‐octane	NUM
eurjchem-1358	106	4	sulfonic	sulfonic	ADJ
eurjchem-1358	106	5	acid	acid	NOUN
eurjchem-1358	106	6	sodium	sodium	NOUN
eurjchem-1358	106	7	salt	salt	NOUN
eurjchem-1358	106	8	monohydrate	monohydrate	NOUN
eurjchem-1358	106	9	as	as	ADP
eurjchem-1358	106	10	ion	ion	NOUN
eurjchem-1358	106	11	pairing	pairing	NOUN
eurjchem-1358	106	12	reagents	reagent	NOUN
eurjchem-1358	106	13	in	in	ADP
eurjchem-1358	106	14	the	the	DET
eurjchem-1358	106	15	aqueous	aqueous	ADJ
eurjchem-1358	106	16	phase	phase	NOUN
eurjchem-1358	106	17	were	be	AUX
eurjchem-1358	106	18	tried	try	VERB
eurjchem-1358	106	19	to	to	PART
eurjchem-1358	106	20	control	control	VERB
eurjchem-1358	106	21	the	the	DET
eurjchem-1358	106	22	tailing	tailing	NOUN
eurjchem-1358	106	23	but	but	CCONJ
eurjchem-1358	106	24	this	this	PRON
eurjchem-1358	106	25	did	do	AUX
eurjchem-1358	106	26	not	not	PART
eurjchem-1358	106	27	give	give	VERB
eurjchem-1358	106	28	a	a	DET
eurjchem-1358	106	29	satisfactory	satisfactory	ADJ
eurjchem-1358	106	30	peaks	peak	NOUN
eurjchem-1358	106	31	tailing	tail	VERB
eurjchem-1358	106	32	factor	factor	NOUN
eurjchem-1358	106	33	.	.	PUNCT
eurjchem-1358	107	1	the	the	DET
eurjchem-1358	107	2	separation	separation	NOUN
eurjchem-1358	107	3	was	be	AUX
eurjchem-1358	107	4	investigated	investigate	VERB
eurjchem-1358	107	5	using	use	VERB
eurjchem-1358	107	6	mobile	mobile	ADJ
eurjchem-1358	107	7	phases	phase	NOUN
eurjchem-1358	107	8	containing	contain	VERB
eurjchem-1358	107	9	(	(	PUNCT
eurjchem-1358	107	10	30	30	NUM
eurjchem-1358	107	11	and	and	CCONJ
eurjchem-1358	107	12	40	40	NUM
eurjchem-1358	107	13	%	%	NOUN
eurjchem-1358	107	14	)	)	PUNCT
eurjchem-1358	107	15	of	of	ADP
eurjchem-1358	107	16	acetonitrile	acetonitrile	NOUN
eurjchem-1358	107	17	with	with	ADP
eurjchem-1358	107	18	phosphate	phosphate	ADJ
eurjchem-1358	107	19	buffer	buffer	NOUN
eurjchem-1358	107	20	with	with	ADP
eurjchem-1358	107	21	different	different	ADJ
eurjchem-1358	107	22	ph	ph	NOUN
eurjchem-1358	107	23	’s	’s	PART
eurjchem-1358	107	24	(	(	PUNCT
eurjchem-1358	107	25	3.0	3.0	NUM
eurjchem-1358	107	26	,	,	PUNCT
eurjchem-1358	107	27	4.5	4.5	NUM
eurjchem-1358	107	28	,	,	PUNCT
eurjchem-1358	107	29	and	and	CCONJ
eurjchem-1358	107	30	6.5	6.5	NUM
eurjchem-1358	107	31	)	)	PUNCT
eurjchem-1358	107	32	.	.	PUNCT
eurjchem-1358	108	1	it	it	PRON
eurjchem-1358	108	2	was	be	AUX
eurjchem-1358	108	3	found	find	VERB
eurjchem-1358	108	4	that	that	SCONJ
eurjchem-1358	108	5	peak	peak	NOUN
eurjchem-1358	108	6	skewing	skewing	NOUN
eurjchem-1358	108	7	occurred	occur	VERB
eurjchem-1358	108	8	with	with	ADP
eurjchem-1358	108	9	increasing	increase	VERB
eurjchem-1358	108	10	the	the	DET
eurjchem-1358	108	11	ratio	ratio	NOUN
eurjchem-1358	108	12	of	of	ADP
eurjchem-1358	108	13	acetonitrile	acetonitrile	NOUN
eurjchem-1358	108	14	in	in	ADP
eurjchem-1358	108	15	the	the	DET
eurjchem-1358	108	16	mobile	mobile	ADJ
eurjchem-1358	108	17	phase	phase	NOUN
eurjchem-1358	108	18	while	while	SCONJ
eurjchem-1358	108	19	it	it	PRON
eurjchem-1358	108	20	had	have	VERB
eurjchem-1358	108	21	slight	slight	ADJ
eurjchem-1358	108	22	decreasing	decrease	VERB
eurjchem-1358	108	23	effect	effect	NOUN
eurjchem-1358	108	24	on	on	ADP
eurjchem-1358	108	25	the	the	DET
eurjchem-1358	108	26	retention	retention	NOUN
eurjchem-1358	108	27	time	time	NOUN
eurjchem-1358	108	28	.	.	PUNCT
eurjchem-1358	109	1	a	a	DET
eurjchem-1358	109	2	mobile	mobile	ADJ
eurjchem-1358	109	3	phase	phase	NOUN
eurjchem-1358	109	4	containing	contain	VERB
eurjchem-1358	109	5	70	70	NUM
eurjchem-1358	109	6	%	%	NOUN
eurjchem-1358	109	7	acetonitrile	acetonitrile	NOUN
eurjchem-1358	109	8	was	be	AUX
eurjchem-1358	109	9	enough	enough	ADJ
eurjchem-1358	109	10	to	to	PART
eurjchem-1358	109	11	give	give	VERB
eurjchem-1358	109	12	sharp	sharp	ADJ
eurjchem-1358	109	13	symmetric	symmetric	ADJ
eurjchem-1358	109	14	peaks	peak	NOUN
eurjchem-1358	109	15	within	within	ADP
eurjchem-1358	109	16	a	a	DET
eurjchem-1358	109	17	short	short	ADJ
eurjchem-1358	109	18	runtime	runtime	NOUN
eurjchem-1358	109	19	with	with	ADP
eurjchem-1358	109	20	reasonable	reasonable	ADJ
eurjchem-1358	109	21	resolution	resolution	NOUN
eurjchem-1358	109	22	and	and	CCONJ
eurjchem-1358	109	23	sensitivity	sensitivity	NOUN
eurjchem-1358	109	24	.	.	PUNCT
eurjchem-1358	110	1	the	the	DET
eurjchem-1358	110	2	separation	separation	NOUN
eurjchem-1358	110	3	was	be	AUX
eurjchem-1358	110	4	investigated	investigate	VERB
eurjchem-1358	110	5	using	use	VERB
eurjchem-1358	110	6	mobile	mobile	ADJ
eurjchem-1358	110	7	phases	phase	NOUN
eurjchem-1358	110	8	containing	contain	VERB
eurjchem-1358	110	9	(	(	PUNCT
eurjchem-1358	110	10	50	50	NUM
eurjchem-1358	110	11	,	,	PUNCT
eurjchem-1358	110	12	60	60	NUM
eurjchem-1358	110	13	,	,	PUNCT
eurjchem-1358	110	14	and	and	CCONJ
eurjchem-1358	110	15	70	70	NUM
eurjchem-1358	110	16	%	%	NOUN
eurjchem-1358	110	17	)	)	PUNCT
eurjchem-1358	110	18	of	of	ADP
eurjchem-1358	110	19	phosphate	phosphate	ADJ
eurjchem-1358	110	20	buffer	buffer	NOUN
eurjchem-1358	110	21	(	(	PUNCT
eurjchem-1358	110	22	ph	ph	NOUN
eurjchem-1358	110	23	=	=	NOUN
eurjchem-1358	110	24	3.0	3.0	NUM
eurjchem-1358	110	25	)	)	PUNCT
eurjchem-1358	110	26	.	.	PUNCT
eurjchem-1358	111	1	it	it	PRON
eurjchem-1358	111	2	was	be	AUX
eurjchem-1358	111	3	found	find	VERB
eurjchem-1358	111	4	increasing	increase	VERB
eurjchem-1358	111	5	the	the	DET
eurjchem-1358	111	6	ratio	ratio	NOUN
eurjchem-1358	111	7	of	of	ADP
eurjchem-1358	111	8	the	the	DET
eurjchem-1358	111	9	buffer	buffer	NOUN
eurjchem-1358	111	10	lead	lead	NOUN
eurjchem-1358	111	11	to	to	PART
eurjchem-1358	111	12	longer	long	ADV
eurjchem-1358	111	13	run	run	VERB
eurjchem-1358	111	14	times	time	NOUN
eurjchem-1358	111	15	with	with	ADP
eurjchem-1358	111	16	broad	broad	ADJ
eurjchem-1358	111	17	peaks	peak	NOUN
eurjchem-1358	111	18	,	,	PUNCT
eurjchem-1358	111	19	as	as	SCONJ
eurjchem-1358	111	20	phosphate	phosphate	ADJ
eurjchem-1358	111	21	buffer	buffer	NOUN
eurjchem-1358	111	22	lead	lead	NOUN
eurjchem-1358	111	23	to	to	ADP
eurjchem-1358	111	24	inadequate	inadequate	ADJ
eurjchem-1358	111	25	resolution	resolution	NOUN
eurjchem-1358	111	26	between	between	ADP
eurjchem-1358	111	27	ob	ob	NOUN
eurjchem-1358	111	28	and	and	CCONJ
eurjchem-1358	111	29	its	its	PRON
eurjchem-1358	111	30	degradation	degradation	NOUN
eurjchem-1358	111	31	product	product	NOUN
eurjchem-1358	111	32	,	,	PUNCT
eurjchem-1358	111	33	finally	finally	ADV
eurjchem-1358	111	34	when	when	SCONJ
eurjchem-1358	111	35	acetate	acetate	NOUN
eurjchem-1358	111	36	buffer	buffer	NOUN
eurjchem-1358	111	37	was	be	AUX
eurjchem-1358	111	38	tried	try	VERB
eurjchem-1358	111	39	(	(	PUNCT
eurjchem-1358	111	40	30	30	NUM
eurjchem-1358	111	41	%	%	NOUN
eurjchem-1358	111	42	)	)	PUNCT
eurjchem-1358	111	43	ph	ph	NOUN
eurjchem-1358	111	44	=	=	NOUN
eurjchem-1358	111	45	2.35	2.35	NUM
eurjchem-1358	111	46	with	with	ADP
eurjchem-1358	111	47	acetonitrile	acetonitrile	NOUN
eurjchem-1358	111	48	(	(	PUNCT
eurjchem-1358	111	49	70	70	NUM
eurjchem-1358	111	50	%	%	NOUN
eurjchem-1358	111	51	)	)	PUNCT
eurjchem-1358	111	52	,	,	PUNCT
eurjchem-1358	111	53	it	it	PRON
eurjchem-1358	111	54	gave	give	VERB
eurjchem-1358	111	55	sharp	sharp	ADJ
eurjchem-1358	111	56	peak	peak	NOUN
eurjchem-1358	111	57	with	with	ADP
eurjchem-1358	111	58	shorter	short	ADJ
eurjchem-1358	111	59	run	run	NOUN
eurjchem-1358	111	60	time	time	NOUN
eurjchem-1358	111	61	.	.	PUNCT
eurjchem-1358	112	1	the	the	DET
eurjchem-1358	112	2	mobile	mobile	ADJ
eurjchem-1358	112	3	phase	phase	NOUN
eurjchem-1358	112	4	was	be	AUX
eurjchem-1358	112	5	pumped	pump	VERB
eurjchem-1358	112	6	at	at	ADP
eurjchem-1358	112	7	a	a	DET
eurjchem-1358	112	8	flow	flow	NOUN
eurjchem-1358	112	9	rate	rate	NOUN
eurjchem-1358	112	10	of	of	ADP
eurjchem-1358	112	11	0.8	0.8	NUM
eurjchem-1358	112	12	ml	ml	NOUN
eurjchem-1358	112	13	/	/	SYM
eurjchem-1358	112	14	min	min	NOUN
eurjchem-1358	112	15	which	which	PRON
eurjchem-1358	112	16	was	be	AUX
eurjchem-1358	112	17	suitable	suitable	ADJ
eurjchem-1358	112	18	for	for	ADP
eurjchem-1358	112	19	good	good	ADJ
eurjchem-1358	112	20	separation	separation	NOUN
eurjchem-1358	112	21	within	within	ADP
eurjchem-1358	112	22	a	a	DET
eurjchem-1358	112	23	reasonable	reasonable	ADJ
eurjchem-1358	112	24	time	time	NOUN
eurjchem-1358	112	25	.	.	PUNCT
eurjchem-1358	113	1	the	the	DET
eurjchem-1358	113	2	chromatographic	chromatographic	ADJ
eurjchem-1358	113	3	separation	separation	NOUN
eurjchem-1358	113	4	was	be	AUX
eurjchem-1358	113	5	tried	try	VERB
eurjchem-1358	113	6	using	use	VERB
eurjchem-1358	113	7	discovery	discovery	NOUN
eurjchem-1358	113	8	cyano	cyano	NOUN
eurjchem-1358	113	9	column	column	NOUN
eurjchem-1358	113	10	(	(	PUNCT
eurjchem-1358	113	11	supelco	supelco	NOUN
eurjchem-1358	113	12	)	)	PUNCT
eurjchem-1358	113	13	with	with	ADP
eurjchem-1358	113	14	dimension	dimension	NOUN
eurjchem-1358	113	15	(	(	PUNCT
eurjchem-1358	113	16	15	15	NUM
eurjchem-1358	113	17	cm	cm	NOUN
eurjchem-1358	113	18	×	×	NOUN
eurjchem-1358	113	19	4.6	4.6	NUM
eurjchem-1358	113	20	mm	mm	NOUN
eurjchem-1358	113	21	,	,	PUNCT
eurjchem-1358	113	22	5	5	NUM
eurjchem-1358	113	23	µm	µm	NOUN
eurjchem-1358	113	24	)	)	PUNCT
eurjchem-1358	113	25	and	and	CCONJ
eurjchem-1358	113	26	hypersil	hypersil	NOUN
eurjchem-1358	113	27	bds	bds	NOUN
eurjchem-1358	113	28	c18	c18	NOUN
eurjchem-1358	113	29	(	(	PUNCT
eurjchem-1358	113	30	15	15	NUM
eurjchem-1358	113	31	cm	cm	NOUN
eurjchem-1358	113	32	×	×	NOUN
eurjchem-1358	113	33	4.6	4.6	NUM
eurjchem-1358	113	34	mm	mm	NOUN
eurjchem-1358	113	35	,	,	PUNCT
eurjchem-1358	113	36	5	5	NUM
eurjchem-1358	113	37	µm	µm	NOUN
eurjchem-1358	113	38	)	)	PUNCT
eurjchem-1358	113	39	.	.	PUNCT
eurjchem-1358	114	1	however	however	ADV
eurjchem-1358	114	2	,	,	PUNCT
eurjchem-1358	114	3	serious	serious	ADJ
eurjchem-1358	114	4	problems	problem	NOUN
eurjchem-1358	114	5	occurred	occur	VERB
eurjchem-1358	114	6	in	in	ADP
eurjchem-1358	114	7	the	the	DET
eurjchem-1358	114	8	determination	determination	NOUN
eurjchem-1358	114	9	of	of	ADP
eurjchem-1358	114	10	ob	ob	NOUN
eurjchem-1358	114	11	,	,	PUNCT
eurjchem-1358	114	12	in	in	ADP
eurjchem-1358	114	13	particular	particular	ADJ
eurjchem-1358	114	14	excessively	excessively	ADV
eurjchem-1358	114	15	tailed	tail	VERB
eurjchem-1358	114	16	peaks	peak	NOUN
eurjchem-1358	114	17	,	,	PUNCT
eurjchem-1358	114	18	due	due	ADP
eurjchem-1358	114	19	to	to	ADP
eurjchem-1358	114	20	its	its	PRON
eurjchem-1358	114	21	quaternary	quaternary	ADJ
eurjchem-1358	114	22	ammonium	ammonium	NOUN
eurjchem-1358	114	23	nature	nature	NOUN
eurjchem-1358	114	24	.	.	PUNCT
eurjchem-1358	115	1	inadequate	inadequate	ADJ
eurjchem-1358	115	2	resolution	resolution	NOUN
eurjchem-1358	115	3	,	,	PUNCT
eurjchem-1358	115	4	broad	broad	ADJ
eurjchem-1358	115	5	peak	peak	NOUN
eurjchem-1358	115	6	and	and	CCONJ
eurjchem-1358	115	7	long	long	ADJ
eurjchem-1358	115	8	retention	retention	NOUN
eurjchem-1358	115	9	time	time	NOUN
eurjchem-1358	115	10	were	be	AUX
eurjchem-1358	115	11	obtained	obtain	VERB
eurjchem-1358	115	12	with	with	ADP
eurjchem-1358	115	13	the	the	DET
eurjchem-1358	115	14	previous	previous	ADJ
eurjchem-1358	115	15	columns	column	NOUN
eurjchem-1358	115	16	.	.	PUNCT
eurjchem-1358	116	1	but	but	CCONJ
eurjchem-1358	116	2	using	use	VERB
eurjchem-1358	116	3	waters	water	NOUN
eurjchem-1358	116	4	atlantis	atlantis	PROPN
eurjchem-1358	116	5	c18	c18	PROPN
eurjchem-1358	116	6	column	column	NOUN
eurjchem-1358	116	7	(	(	PUNCT
eurjchem-1358	116	8	4.6	4.6	NUM
eurjchem-1358	116	9	×	×	NOUN
eurjchem-1358	116	10	150	150	NUM
eurjchem-1358	116	11	mm	mm	NOUN
eurjchem-1358	116	12	,	,	PUNCT
eurjchem-1358	116	13	5	5	NUM
eurjchem-1358	116	14	µm	µm	NOUN
eurjchem-1358	116	15	)	)	PUNCT
eurjchem-1358	116	16	;	;	PUNCT
eurjchem-1358	116	17	less	less	ADV
eurjchem-1358	116	18	hydrophobic	hydrophobic	NOUN
eurjchem-1358	116	19	column	column	NOUN
eurjchem-1358	116	20	showed	show	VERB
eurjchem-1358	116	21	better	well	ADJ
eurjchem-1358	116	22	peak	peak	NOUN
eurjchem-1358	116	23	shapes	shape	NOUN
eurjchem-1358	116	24	within	within	ADP
eurjchem-1358	116	25	reasonable	reasonable	ADJ
eurjchem-1358	116	26	run	run	NOUN
eurjchem-1358	116	27	time	time	NOUN
eurjchem-1358	116	28	and	and	CCONJ
eurjchem-1358	116	29	satisfactory	satisfactory	ADJ
eurjchem-1358	116	30	separation	separation	NOUN
eurjchem-1358	116	31	hence	hence	ADV
eurjchem-1358	116	32	it	it	PRON
eurjchem-1358	116	33	became	become	VERB
eurjchem-1358	116	34	the	the	DET
eurjchem-1358	116	35	column	column	NOUN
eurjchem-1358	116	36	of	of	ADP
eurjchem-1358	116	37	choice	choice	NOUN
eurjchem-1358	116	38	for	for	ADP
eurjchem-1358	116	39	this	this	DET
eurjchem-1358	116	40	study	study	NOUN
eurjchem-1358	116	41	.	.	PUNCT
eurjchem-1358	117	1	detection	detection	NOUN
eurjchem-1358	117	2	was	be	AUX
eurjchem-1358	117	3	tried	try	VERB
eurjchem-1358	117	4	at	at	ADP
eurjchem-1358	117	5	224	224	NUM
eurjchem-1358	117	6	,	,	PUNCT
eurjchem-1358	117	7	254	254	NUM
eurjchem-1358	117	8	and	and	CCONJ
eurjchem-1358	117	9	290	290	NUM
eurjchem-1358	117	10	nm	nm	NOUN
eurjchem-1358	117	11	but	but	CCONJ
eurjchem-1358	117	12	finally	finally	ADV
eurjchem-1358	117	13	290	290	NUM
eurjchem-1358	117	14	nm	nm	NOUN
eurjchem-1358	117	15	was	be	AUX
eurjchem-1358	117	16	chosen	choose	VERB
eurjchem-1358	117	17	as	as	SCONJ
eurjchem-1358	117	18	it	it	PRON
eurjchem-1358	117	19	was	be	AUX
eurjchem-1358	117	20	found	find	VERB
eurjchem-1358	117	21	optimum	optimum	ADJ
eurjchem-1358	117	22	for	for	ADP
eurjchem-1358	117	23	measurements	measurement	NOUN
eurjchem-1358	117	24	.	.	PUNCT
eurjchem-1358	118	1	3.2	3.2	NUM
eurjchem-1358	118	2	.	.	PUNCT
eurjchem-1358	119	1	system	system	NOUN
eurjchem-1358	119	2	suitability	suitability	NOUN
eurjchem-1358	119	3	tests	test	VERB
eurjchem-1358	119	4	the	the	DET
eurjchem-1358	119	5	system	system	NOUN
eurjchem-1358	119	6	suitability	suitability	NOUN
eurjchem-1358	119	7	tests	test	NOUN
eurjchem-1358	119	8	were	be	AUX
eurjchem-1358	119	9	performed	perform	VERB
eurjchem-1358	119	10	to	to	PART
eurjchem-1358	119	11	ensure	ensure	VERB
eurjchem-1358	119	12	that	that	SCONJ
eurjchem-1358	119	13	the	the	DET
eurjchem-1358	119	14	proposed	propose	VERB
eurjchem-1358	119	15	lc	lc	NOUN
eurjchem-1358	119	16	method	method	NOUN
eurjchem-1358	119	17	was	be	AUX
eurjchem-1358	119	18	suitable	suitable	ADJ
eurjchem-1358	119	19	to	to	ADP
eurjchem-1358	119	20	the	the	DET
eurjchem-1358	119	21	analysis	analysis	NOUN
eurjchem-1358	119	22	intended	intend	VERB
eurjchem-1358	119	23	.	.	PUNCT
eurjchem-1358	120	1	the	the	DET
eurjchem-1358	120	2	parameters	parameter	NOUN
eurjchem-1358	120	3	of	of	ADP
eurjchem-1358	120	4	these	these	DET
eurjchem-1358	120	5	tests	test	NOUN
eurjchem-1358	120	6	are	be	AUX
eurjchem-1358	120	7	column	column	NOUN
eurjchem-1358	120	8	efficiency	efficiency	NOUN
eurjchem-1358	120	9	(	(	PUNCT
eurjchem-1358	120	10	number	number	NOUN
eurjchem-1358	120	11	of	of	ADP
eurjchem-1358	120	12	theoretical	theoretical	ADJ
eurjchem-1358	120	13	plates	plate	NOUN
eurjchem-1358	120	14	)	)	PUNCT
eurjchem-1358	120	15	,	,	PUNCT
eurjchem-1358	120	16	tailing	tail	VERB
eurjchem-1358	120	17	of	of	ADP
eurjchem-1358	120	18	chromatographic	chromatographic	ADJ
eurjchem-1358	120	19	peak	peak	NOUN
eurjchem-1358	120	20	,	,	PUNCT
eurjchem-1358	120	21	repeatability	repeatability	NOUN
eurjchem-1358	120	22	as	as	ADP
eurjchem-1358	120	23	%	%	ADP
eurjchem-1358	120	24	r.s.d	r.s.d	NOUN
eurjchem-1358	120	25	of	of	ADP
eurjchem-1358	120	26	peak	peak	NOUN
eurjchem-1358	120	27	area	area	NOUN
eurjchem-1358	120	28	for	for	ADP
eurjchem-1358	120	29	six	six	NUM
eurjchem-1358	120	30	injections	injection	NOUN
eurjchem-1358	120	31	and	and	CCONJ
eurjchem-1358	120	32	reproducibility	reproducibility	NOUN
eurjchem-1358	120	33	of	of	ADP
eurjchem-1358	120	34	retention	retention	NOUN
eurjchem-1358	120	35	as	as	ADP
eurjchem-1358	120	36	%	%	INTJ
eurjchem-1358	120	37	r.s.d	r.s.d	NOUN
eurjchem-1358	120	38	of	of	ADP
eurjchem-1358	120	39	retention	retention	NOUN
eurjchem-1358	120	40	time	time	NOUN
eurjchem-1358	120	41	of	of	ADP
eurjchem-1358	120	42	a	a	DET
eurjchem-1358	120	43	solution	solution	NOUN
eurjchem-1358	120	44	of	of	ADP
eurjchem-1358	120	45	a	a	DET
eurjchem-1358	120	46	50	50	NUM
eurjchem-1358	120	47	µg	µg	NOUN
eurjchem-1358	120	48	/	/	SYM
eurjchem-1358	120	49	ml	ml	NOUN
eurjchem-1358	120	50	of	of	ADP
eurjchem-1358	120	51	ob	ob	X
eurjchem-1358	120	52	(	(	PUNCT
eurjchem-1358	120	53	100	100	NUM
eurjchem-1358	120	54	%	%	NOUN
eurjchem-1358	120	55	concentration	concentration	NOUN
eurjchem-1358	120	56	)	)	PUNCT
eurjchem-1358	120	57	and	and	CCONJ
eurjchem-1358	120	58	25	25	NUM
eurjchem-1358	120	59	µg	µg	NOUN
eurjchem-1358	120	60	/	/	SYM
eurjchem-1358	120	61	ml	ml	NOUN
eurjchem-1358	120	62	of	of	ADP
eurjchem-1358	120	63	its	its	PRON
eurjchem-1358	120	64	degradant	degradant	NOUN
eurjchem-1358	120	65	.	.	PUNCT
eurjchem-1358	121	1	the	the	DET
eurjchem-1358	121	2	results	result	NOUN
eurjchem-1358	121	3	of	of	ADP
eurjchem-1358	121	4	these	these	DET
eurjchem-1358	121	5	tests	test	NOUN
eurjchem-1358	121	6	for	for	ADP
eurjchem-1358	121	7	the	the	DET
eurjchem-1358	121	8	proposed	propose	VERB
eurjchem-1358	121	9	method	method	NOUN
eurjchem-1358	121	10	are	be	AUX
eurjchem-1358	121	11	listed	list	VERB
eurjchem-1358	121	12	in	in	ADP
eurjchem-1358	121	13	table	table	NOUN
eurjchem-1358	121	14	1	1	NUM
eurjchem-1358	121	15	.	.	ADP
eurjchem-1358	121	16	3.3	3.3	NUM
eurjchem-1358	121	17	.	.	PUNCT
eurjchem-1358	122	1	method	method	NOUN
eurjchem-1358	122	2	validation	validation	NOUN
eurjchem-1358	122	3	3.3.1	3.3.1	PROPN
eurjchem-1358	122	4	.	.	PUNCT
eurjchem-1358	122	5	linearity	linearity	NOUN
eurjchem-1358	122	6	in	in	ADP
eurjchem-1358	122	7	this	this	DET
eurjchem-1358	122	8	study	study	NOUN
eurjchem-1358	122	9	,	,	PUNCT
eurjchem-1358	122	10	eight	eight	NUM
eurjchem-1358	122	11	concentrations	concentration	NOUN
eurjchem-1358	122	12	were	be	AUX
eurjchem-1358	122	13	chosen	choose	VERB
eurjchem-1358	122	14	for	for	ADP
eurjchem-1358	122	15	ob	ob	NUM
eurjchem-1358	122	16	and	and	CCONJ
eurjchem-1358	122	17	six	six	NUM
eurjchem-1358	122	18	concentrations	concentration	NOUN
eurjchem-1358	122	19	were	be	AUX
eurjchem-1358	122	20	chosen	choose	VERB
eurjchem-1358	122	21	for	for	ADP
eurjchem-1358	122	22	paba	paba	PROPN
eurjchem-1358	122	23	.	.	PUNCT
eurjchem-1358	123	1	each	each	DET
eurjchem-1358	123	2	concentration	concentration	NOUN
eurjchem-1358	123	3	was	be	AUX
eurjchem-1358	123	4	analyzed	analyze	VERB
eurjchem-1358	123	5	three	three	NUM
eurjchem-1358	123	6	times	time	NOUN
eurjchem-1358	123	7	and	and	CCONJ
eurjchem-1358	123	8	linearity	linearity	NOUN
eurjchem-1358	123	9	was	be	AUX
eurjchem-1358	123	10	studied	study	VERB
eurjchem-1358	123	11	for	for	ADP
eurjchem-1358	123	12	both	both	DET
eurjchem-1358	123	13	drugs	drug	NOUN
eurjchem-1358	123	14	.	.	PUNCT
eurjchem-1358	124	1	a	a	DET
eurjchem-1358	124	2	linear	linear	ADJ
eurjchem-1358	124	3	relationship	relationship	NOUN
eurjchem-1358	124	4	between	between	ADP
eurjchem-1358	124	5	area	area	NOUN
eurjchem-1358	124	6	under	under	ADP
eurjchem-1358	124	7	the	the	DET
eurjchem-1358	124	8	peak	peak	NOUN
eurjchem-1358	124	9	(	(	PUNCT
eurjchem-1358	124	10	aup	aup	PROPN
eurjchem-1358	124	11	)	)	PUNCT
eurjchem-1358	124	12	and	and	CCONJ
eurjchem-1358	124	13	concentrations	concentration	NOUN
eurjchem-1358	124	14	(	(	PUNCT
eurjchem-1358	124	15	c	c	X
eurjchem-1358	124	16	)	)	PUNCT
eurjchem-1358	124	17	was	be	AUX
eurjchem-1358	124	18	obtained	obtain	VERB
eurjchem-1358	124	19	and	and	CCONJ
eurjchem-1358	124	20	the	the	DET
eurjchem-1358	124	21	regression	regression	NOUN
eurjchem-1358	124	22	equation	equation	NOUN
eurjchem-1358	124	23	for	for	ADP
eurjchem-1358	124	24	ob	ob	PRON
eurjchem-1358	124	25	and	and	CCONJ
eurjchem-1358	124	26	paba	paba	PROPN
eurjchem-1358	124	27	was	be	AUX
eurjchem-1358	124	28	computed	compute	VERB
eurjchem-1358	124	29	,	,	PUNCT
eurjchem-1358	124	30	table	table	NOUN
eurjchem-1358	124	31	2	2	NUM
eurjchem-1358	124	32	.	.	PUNCT
eurjchem-1358	125	1	the	the	DET
eurjchem-1358	125	2	linearity	linearity	NOUN
eurjchem-1358	125	3	of	of	ADP
eurjchem-1358	125	4	the	the	DET
eurjchem-1358	125	5	calibration	calibration	NOUN
eurjchem-1358	125	6	curve	curve	NOUN
eurjchem-1358	125	7	was	be	AUX
eurjchem-1358	125	8	validated	validate	VERB
eurjchem-1358	125	9	by	by	ADP
eurjchem-1358	125	10	the	the	DET
eurjchem-1358	125	11	high	high	ADJ
eurjchem-1358	125	12	value	value	NOUN
eurjchem-1358	125	13	of	of	ADP
eurjchem-1358	125	14	correlation	correlation	NOUN
eurjchem-1358	125	15	coefficient	coefficient	NOUN
eurjchem-1358	125	16	.	.	PUNCT
eurjchem-1358	126	1	3.3.2	3.3.2	NUM
eurjchem-1358	126	2	.	.	PUNCT
eurjchem-1358	126	3	accuracy	accuracy	NOUN
eurjchem-1358	126	4	accuracy	accuracy	NOUN
eurjchem-1358	126	5	of	of	ADP
eurjchem-1358	126	6	the	the	DET
eurjchem-1358	126	7	results	result	NOUN
eurjchem-1358	126	8	was	be	AUX
eurjchem-1358	126	9	calculated	calculate	VERB
eurjchem-1358	126	10	by	by	ADP
eurjchem-1358	126	11	%	%	NOUN
eurjchem-1358	126	12	recovery	recovery	NOUN
eurjchem-1358	126	13	of	of	ADP
eurjchem-1358	126	14	6	6	NUM
eurjchem-1358	126	15	concentrations	concentration	NOUN
eurjchem-1358	126	16	(	(	PUNCT
eurjchem-1358	126	17	injected	inject	VERB
eurjchem-1358	126	18	in	in	ADP
eurjchem-1358	126	19	triplicates	triplicate	NOUN
eurjchem-1358	126	20	)	)	PUNCT
eurjchem-1358	126	21	of	of	ADP
eurjchem-1358	126	22	ob	ob	NOUN
eurjchem-1358	126	23	and	and	CCONJ
eurjchem-1358	126	24	paba	paba	NOUN
eurjchem-1358	126	25	in	in	ADP
eurjchem-1358	126	26	bulk	bulk	ADJ
eurjchem-1358	126	27	powder	powder	NOUN
eurjchem-1358	126	28	and	and	CCONJ
eurjchem-1358	126	29	in	in	ADP
eurjchem-1358	126	30	mixtures	mixture	NOUN
eurjchem-1358	126	31	,	,	PUNCT
eurjchem-1358	126	32	and	and	CCONJ
eurjchem-1358	126	33	also	also	ADV
eurjchem-1358	126	34	by	by	ADP
eurjchem-1358	126	35	standard	standard	ADJ
eurjchem-1358	126	36	addition	addition	NOUN
eurjchem-1358	126	37	technique	technique	NOUN
eurjchem-1358	126	38	applied	apply	VERB
eurjchem-1358	126	39	to	to	ADP
eurjchem-1358	126	40	spasmomen	spasmoman	NOUN
eurjchem-1358	126	41	®	®	NOUN
eurjchem-1358	126	42	40	40	NUM
eurjchem-1358	126	43	mg	mg	NOUN
eurjchem-1358	126	44	.	.	PUNCT
eurjchem-1358	127	1	the	the	DET
eurjchem-1358	127	2	results	result	NOUN
eurjchem-1358	127	3	obtained	obtain	VERB
eurjchem-1358	127	4	are	be	AUX
eurjchem-1358	127	5	displayed	display	VERB
eurjchem-1358	127	6	in	in	ADP
eurjchem-1358	127	7	table	table	NOUN
eurjchem-1358	127	8	2	2	NUM
eurjchem-1358	127	9	.	.	X
eurjchem-1358	128	1	3.3.3	3.3.3	NUM
eurjchem-1358	128	2	.	.	PUNCT
eurjchem-1358	128	3	precision	precision	VERB
eurjchem-1358	128	4	the	the	DET
eurjchem-1358	128	5	repeatability	repeatability	NOUN
eurjchem-1358	128	6	(	(	PUNCT
eurjchem-1358	128	7	intra‐day	intra‐day	NOUN
eurjchem-1358	128	8	)	)	PUNCT
eurjchem-1358	128	9	was	be	AUX
eurjchem-1358	128	10	assessed	assess	VERB
eurjchem-1358	128	11	by	by	ADP
eurjchem-1358	128	12	three	three	NUM
eurjchem-1358	128	13	determinations	determination	NOUN
eurjchem-1358	128	14	for	for	ADP
eurjchem-1358	128	15	each	each	DET
eurjchem-1358	128	16	concentration	concentration	NOUN
eurjchem-1358	128	17	(	(	PUNCT
eurjchem-1358	128	18	40	40	NUM
eurjchem-1358	128	19	,	,	PUNCT
eurjchem-1358	128	20	50	50	NUM
eurjchem-1358	128	21	and	and	CCONJ
eurjchem-1358	128	22	60	60	NUM
eurjchem-1358	128	23	µg	µg	ADV
eurjchem-1358	128	24	/	/	SYM
eurjchem-1358	128	25	ml	ml	NOUN
eurjchem-1358	128	26	)	)	PUNCT
eurjchem-1358	128	27	for	for	ADP
eurjchem-1358	128	28	ob	ob	NOUN
eurjchem-1358	128	29	and	and	CCONJ
eurjchem-1358	128	30	(	(	PUNCT
eurjchem-1358	128	31	20	20	NUM
eurjchem-1358	128	32	,	,	PUNCT
eurjchem-1358	128	33	25	25	NUM
eurjchem-1358	128	34	and	and	CCONJ
eurjchem-1358	128	35	30	30	NUM
eurjchem-1358	128	36	µg	µg	NOUN
eurjchem-1358	128	37	/	/	SYM
eurjchem-1358	128	38	ml	ml	NOUN
eurjchem-1358	128	39	)	)	PUNCT
eurjchem-1358	128	40	for	for	ADP
eurjchem-1358	128	41	paba	paba	NOUN
eurjchem-1358	128	42	representing	represent	VERB
eurjchem-1358	128	43	80	80	NUM
eurjchem-1358	128	44	,	,	PUNCT
eurjchem-1358	128	45	100	100	NUM
eurjchem-1358	128	46	and	and	CCONJ
eurjchem-1358	128	47	120	120	NUM
eurjchem-1358	128	48	%	%	NOUN
eurjchem-1358	128	49	,	,	PUNCT
eurjchem-1358	128	50	respectively	respectively	ADV
eurjchem-1358	128	51	.	.	PUNCT
eurjchem-1358	129	1	100	100	NUM
eurjchem-1358	129	2	el‐kerdawy	el‐kerdawy	PROPN
eurjchem-1358	129	3	et	et	PROPN
eurjchem-1358	129	4	al	al	PROPN
eurjchem-1358	129	5	.	.	PUNCT
eurjchem-1358	129	6	/	/	SYM
eurjchem-1358	129	7	european	european	PROPN
eurjchem-1358	129	8	journal	journal	PROPN
eurjchem-1358	129	9	of	of	ADP
eurjchem-1358	129	10	chemistry	chemistry	NOUN
eurjchem-1358	129	11	7	7	NUM
eurjchem-1358	129	12	(	(	PUNCT
eurjchem-1358	129	13	1	1	NUM
eurjchem-1358	129	14	)	)	PUNCT
eurjchem-1358	129	15	(	(	PUNCT
eurjchem-1358	129	16	2016	2016	NUM
eurjchem-1358	129	17	)	)	PUNCT
eurjchem-1358	129	18	97‐101	97‐101	PROPN
eurjchem-1358	129	19	table	table	NOUN
eurjchem-1358	129	20	3	3	NUM
eurjchem-1358	129	21	.	.	X
eurjchem-1358	129	22	results	result	NOUN
eurjchem-1358	129	23	for	for	ADP
eurjchem-1358	129	24	determination	determination	NOUN
eurjchem-1358	129	25	of	of	ADP
eurjchem-1358	129	26	repeatability	repeatability	NOUN
eurjchem-1358	129	27	of	of	ADP
eurjchem-1358	129	28	ob	ob	NOUN
eurjchem-1358	129	29	in	in	ADP
eurjchem-1358	129	30	powder	powder	NOUN
eurjchem-1358	129	31	and	and	CCONJ
eurjchem-1358	129	32	in	in	ADP
eurjchem-1358	129	33	presence	presence	NOUN
eurjchem-1358	129	34	of	of	ADP
eurjchem-1358	129	35	paba	paba	NOUN
eurjchem-1358	129	36	by	by	ADP
eurjchem-1358	129	37	proposed	propose	VERB
eurjchem-1358	129	38	lc	lc	PROPN
eurjchem-1358	129	39	method	method	NOUN
eurjchem-1358	129	40	.	.	PUNCT
eurjchem-1358	130	1	sample	sample	NOUN
eurjchem-1358	130	2	ob	ob	INTJ
eurjchem-1358	130	3	in	in	ADP
eurjchem-1358	130	4	powder	powder	NOUN
eurjchem-1358	130	5	ob	ob	NOUN
eurjchem-1358	130	6	in	in	ADP
eurjchem-1358	130	7	presence	presence	NOUN
eurjchem-1358	130	8	of	of	ADP
eurjchem-1358	130	9	paba	paba	PROPN
eurjchem-1358	130	10	concentration	concentration	NOUN
eurjchem-1358	130	11	40	40	NUM
eurjchem-1358	130	12	μg	μg	NOUN
eurjchem-1358	130	13	/	/	SYM
eurjchem-1358	130	14	ml	ml	PROPN
eurjchem-1358	130	15	80	80	NUM
eurjchem-1358	130	16	%	%	NOUN
eurjchem-1358	130	17	50	50	NUM
eurjchem-1358	130	18	μg	μg	NOUN
eurjchem-1358	130	19	/	/	SYM
eurjchem-1358	130	20	ml	ml	NOUN
eurjchem-1358	130	21	100	100	NUM
eurjchem-1358	130	22	%	%	NOUN
eurjchem-1358	130	23	60	60	NUM
eurjchem-1358	130	24	μg	μg	NOUN
eurjchem-1358	130	25	/	/	SYM
eurjchem-1358	130	26	ml	ml	NOUN
eurjchem-1358	130	27	120	120	NUM
eurjchem-1358	130	28	%	%	NOUN
eurjchem-1358	130	29	40	40	NUM
eurjchem-1358	130	30	μg	μg	NOUN
eurjchem-1358	130	31	/	/	SYM
eurjchem-1358	130	32	ml	ml	PROPN
eurjchem-1358	130	33	80	80	NUM
eurjchem-1358	130	34	%	%	NOUN
eurjchem-1358	130	35	50	50	NUM
eurjchem-1358	130	36	μg	μg	NOUN
eurjchem-1358	130	37	/	/	SYM
eurjchem-1358	130	38	ml	ml	NOUN
eurjchem-1358	130	39	100	100	NUM
eurjchem-1358	130	40	%	%	NOUN
eurjchem-1358	130	41	60	60	NUM
eurjchem-1358	130	42	μg	μg	NOUN
eurjchem-1358	130	43	/	/	SYM
eurjchem-1358	130	44	ml	ml	NOUN
eurjchem-1358	130	45	120	120	NUM
eurjchem-1358	130	46	%	%	NOUN
eurjchem-1358	130	47	mean	mean	NOUN
eurjchem-1358	130	48	40.8473	40.8473	NUM
eurjchem-1358	130	49	51.0867	51.0867	NUM
eurjchem-1358	130	50	61.0862	61.0862	NUM
eurjchem-1358	130	51	40.8230	40.8230	NUM
eurjchem-1358	130	52	50.7244	50.7244	NUM
eurjchem-1358	130	53	59.6314	59.6314	NUM
eurjchem-1358	130	54	%	%	NOUN
eurjchem-1358	130	55	recovery	recovery	NOUN
eurjchem-1358	130	56	102.12	102.12	NUM
eurjchem-1358	130	57	102.17	102.17	NUM
eurjchem-1358	130	58	101.81	101.81	NUM
eurjchem-1358	130	59	102.06	102.06	NUM
eurjchem-1358	130	60	101.45	101.45	NUM
eurjchem-1358	130	61	99.39	99.39	NUM
eurjchem-1358	130	62	s.d	s.d	PROPN
eurjchem-1358	130	63	.	.	PROPN
eurjchem-1358	131	1	0.1294	0.1294	NUM
eurjchem-1358	131	2	0.2262	0.2262	NUM
eurjchem-1358	131	3	0.2895	0.2895	NUM
eurjchem-1358	131	4	0.1141	0.1141	NUM
eurjchem-1358	131	5	0.2547	0.2547	NUM
eurjchem-1358	131	6	0.6080	0.6080	NUM
eurjchem-1358	131	7	%	%	NOUN
eurjchem-1358	131	8	r.s.d	r.s.d	VERB
eurjchem-1358	131	9	0.3168	0.3168	NUM
eurjchem-1358	131	10	0.4428	0.4428	NUM
eurjchem-1358	131	11	0.4739	0.4739	NUM
eurjchem-1358	131	12	0.2795	0.2795	NUM
eurjchem-1358	131	13	0.5021	0.5021	NUM
eurjchem-1358	131	14	1.0196	1.0196	NUM
eurjchem-1358	131	15	table	table	NOUN
eurjchem-1358	131	16	4	4	NUM
eurjchem-1358	131	17	.	.	NOUN
eurjchem-1358	131	18	results	result	NOUN
eurjchem-1358	131	19	for	for	ADP
eurjchem-1358	131	20	determination	determination	NOUN
eurjchem-1358	131	21	of	of	ADP
eurjchem-1358	131	22	repeatability	repeatability	NOUN
eurjchem-1358	131	23	of	of	ADP
eurjchem-1358	131	24	paba	paba	NOUN
eurjchem-1358	131	25	in	in	ADP
eurjchem-1358	131	26	bulk	bulk	ADJ
eurjchem-1358	131	27	powder	powder	NOUN
eurjchem-1358	131	28	and	and	CCONJ
eurjchem-1358	131	29	in	in	ADP
eurjchem-1358	131	30	presence	presence	NOUN
eurjchem-1358	131	31	of	of	ADP
eurjchem-1358	131	32	ob	ob	NUM
eurjchem-1358	131	33	by	by	ADP
eurjchem-1358	131	34	proposed	propose	VERB
eurjchem-1358	131	35	lc	lc	PROPN
eurjchem-1358	131	36	method	method	NOUN
eurjchem-1358	131	37	.	.	PUNCT
eurjchem-1358	132	1	sample	sample	NOUN
eurjchem-1358	132	2	paba	paba	NOUN
eurjchem-1358	132	3	in	in	ADP
eurjchem-1358	132	4	powder	powder	NOUN
eurjchem-1358	132	5	paba	paba	NOUN
eurjchem-1358	132	6	in	in	ADP
eurjchem-1358	132	7	presence	presence	NOUN
eurjchem-1358	132	8	of	of	ADP
eurjchem-1358	132	9	ob	ob	ADP
eurjchem-1358	132	10	concentration	concentration	NOUN
eurjchem-1358	132	11	20	20	NUM
eurjchem-1358	132	12	μg	μg	NOUN
eurjchem-1358	132	13	/	/	SYM
eurjchem-1358	132	14	ml	ml	NOUN
eurjchem-1358	132	15	80	80	NUM
eurjchem-1358	132	16	%	%	NOUN
eurjchem-1358	132	17	25	25	NUM
eurjchem-1358	132	18	μg	μg	NOUN
eurjchem-1358	132	19	/	/	SYM
eurjchem-1358	132	20	ml	ml	NOUN
eurjchem-1358	132	21	100	100	NUM
eurjchem-1358	132	22	%	%	NOUN
eurjchem-1358	132	23	30	30	NUM
eurjchem-1358	132	24	μg	μg	NOUN
eurjchem-1358	132	25	/	/	SYM
eurjchem-1358	132	26	ml	ml	NOUN
eurjchem-1358	132	27	120	120	NUM
eurjchem-1358	132	28	%	%	NOUN
eurjchem-1358	132	29	20	20	NUM
eurjchem-1358	132	30	μg	μg	NOUN
eurjchem-1358	132	31	/	/	SYM
eurjchem-1358	132	32	ml	ml	NOUN
eurjchem-1358	132	33	80	80	NUM
eurjchem-1358	132	34	%	%	NOUN
eurjchem-1358	132	35	25	25	NUM
eurjchem-1358	132	36	μg	μg	NOUN
eurjchem-1358	132	37	/	/	SYM
eurjchem-1358	132	38	ml	ml	NOUN
eurjchem-1358	132	39	100	100	NUM
eurjchem-1358	132	40	%	%	NOUN
eurjchem-1358	132	41	30	30	NUM
eurjchem-1358	132	42	μg	μg	NOUN
eurjchem-1358	132	43	/	/	SYM
eurjchem-1358	132	44	ml	ml	NOUN
eurjchem-1358	132	45	120	120	NUM
eurjchem-1358	132	46	%	%	NOUN
eurjchem-1358	132	47	mean	mean	NOUN
eurjchem-1358	132	48	19.7837	19.7837	NUM
eurjchem-1358	132	49	24.7078	24.7078	NUM
eurjchem-1358	132	50	29.6433	29.6433	NUM
eurjchem-1358	132	51	19.8655	19.8655	NUM
eurjchem-1358	132	52	24.7974	24.7974	NUM
eurjchem-1358	132	53	29.4563	29.4563	NUM
eurjchem-1358	132	54	%	%	NOUN
eurjchem-1358	132	55	recovery	recovery	NOUN
eurjchem-1358	132	56	98.92	98.92	NUM
eurjchem-1358	132	57	98.83	98.83	NUM
eurjchem-1358	132	58	98.81	98.81	NUM
eurjchem-1358	132	59	99.32	99.32	NUM
eurjchem-1358	132	60	99.19	99.19	NUM
eurjchem-1358	132	61	98.19	98.19	NUM
eurjchem-1358	132	62	s.d	s.d	PROPN
eurjchem-1358	132	63	.	.	PROPN
eurjchem-1358	132	64	0.0876	0.0876	NUM
eurjchem-1358	132	65	0.2096	0.2096	NUM
eurjchem-1358	132	66	0.2019	0.2019	NUM
eurjchem-1358	132	67	0.0706	0.0706	NUM
eurjchem-1358	132	68	0.1302	0.1302	NUM
eurjchem-1358	132	69	0.2587	0.2587	NUM
eurjchem-1358	132	70	%	%	NOUN
eurjchem-1358	132	71	r.s.d	r.s.d	ADP
eurjchem-1358	132	72	0.4429	0.4429	NUM
eurjchem-1358	132	73	0.8481	0.8481	NUM
eurjchem-1358	132	74	0.6809	0.6809	NUM
eurjchem-1358	132	75	0.3556	0.3556	NUM
eurjchem-1358	132	76	0.5251	0.5251	NUM
eurjchem-1358	132	77	0.8782	0.8782	NUM
eurjchem-1358	132	78	table	table	NOUN
eurjchem-1358	132	79	5	5	NUM
eurjchem-1358	132	80	.	.	PUNCT
eurjchem-1358	132	81	results	result	NOUN
eurjchem-1358	132	82	for	for	ADP
eurjchem-1358	132	83	determination	determination	NOUN
eurjchem-1358	132	84	of	of	ADP
eurjchem-1358	132	85	inter‐day	inter‐day	NOUN
eurjchem-1358	132	86	assay	assay	VERB
eurjchem-1358	132	87	for	for	ADP
eurjchem-1358	132	88	ob	ob	NOUN
eurjchem-1358	132	89	in	in	ADP
eurjchem-1358	132	90	bulk	bulk	ADJ
eurjchem-1358	132	91	powder	powder	NOUN
eurjchem-1358	132	92	and	and	CCONJ
eurjchem-1358	132	93	in	in	ADP
eurjchem-1358	132	94	presence	presence	NOUN
eurjchem-1358	132	95	of	of	ADP
eurjchem-1358	132	96	paba	paba	NOUN
eurjchem-1358	132	97	by	by	ADP
eurjchem-1358	132	98	proposed	propose	VERB
eurjchem-1358	132	99	lc	lc	PROPN
eurjchem-1358	132	100	method	method	NOUN
eurjchem-1358	132	101	.	.	PUNCT
eurjchem-1358	133	1	sample	sample	NOUN
eurjchem-1358	133	2	inter‐day	inter‐day	PROPN
eurjchem-1358	133	3	in	in	ADP
eurjchem-1358	133	4	bulk	bulk	ADJ
eurjchem-1358	133	5	powder	powder	NOUN
eurjchem-1358	133	6	inter‐day	inter‐day	NOUN
eurjchem-1358	133	7	in	in	ADP
eurjchem-1358	133	8	presence	presence	NOUN
eurjchem-1358	133	9	of	of	ADP
eurjchem-1358	133	10	paba	paba	PROPN
eurjchem-1358	133	11	concentration	concentration	NOUN
eurjchem-1358	133	12	40	40	NUM
eurjchem-1358	133	13	μg	μg	NOUN
eurjchem-1358	133	14	/	/	SYM
eurjchem-1358	133	15	ml	ml	PROPN
eurjchem-1358	133	16	80	80	NUM
eurjchem-1358	133	17	%	%	NOUN
eurjchem-1358	133	18	50	50	NUM
eurjchem-1358	133	19	μg	μg	NOUN
eurjchem-1358	133	20	/	/	SYM
eurjchem-1358	133	21	ml	ml	NOUN
eurjchem-1358	133	22	100	100	NUM
eurjchem-1358	133	23	%	%	NOUN
eurjchem-1358	133	24	60	60	NUM
eurjchem-1358	133	25	μg	μg	NOUN
eurjchem-1358	133	26	/	/	SYM
eurjchem-1358	133	27	ml	ml	NOUN
eurjchem-1358	133	28	120	120	NUM
eurjchem-1358	133	29	%	%	NOUN
eurjchem-1358	133	30	40	40	NUM
eurjchem-1358	133	31	μg	μg	NOUN
eurjchem-1358	133	32	/	/	SYM
eurjchem-1358	133	33	ml	ml	PROPN
eurjchem-1358	133	34	80	80	NUM
eurjchem-1358	133	35	%	%	NOUN
eurjchem-1358	133	36	50	50	NUM
eurjchem-1358	133	37	μg	μg	NOUN
eurjchem-1358	133	38	/	/	SYM
eurjchem-1358	133	39	ml	ml	NOUN
eurjchem-1358	133	40	100	100	NUM
eurjchem-1358	133	41	%	%	NOUN
eurjchem-1358	133	42	60	60	NUM
eurjchem-1358	133	43	μg	μg	NOUN
eurjchem-1358	133	44	/	/	SYM
eurjchem-1358	133	45	ml	ml	NOUN
eurjchem-1358	133	46	120	120	NUM
eurjchem-1358	133	47	%	%	NOUN
eurjchem-1358	133	48	mean	mean	NOUN
eurjchem-1358	133	49	40.49	40.49	NUM
eurjchem-1358	133	50	50.99	50.99	NUM
eurjchem-1358	133	51	60.39	60.39	NUM
eurjchem-1358	133	52	40.74	40.74	NUM
eurjchem-1358	133	53	50.30	50.30	NUM
eurjchem-1358	133	54	59.76	59.76	NUM
eurjchem-1358	133	55	%	%	NOUN
eurjchem-1358	133	56	recovery	recovery	NOUN
eurjchem-1358	133	57	101.23	101.23	NUM
eurjchem-1358	133	58	101.98	101.98	NUM
eurjchem-1358	133	59	100.65	100.65	NUM
eurjchem-1358	133	60	101.85	101.85	NUM
eurjchem-1358	133	61	100.60	100.60	NUM
eurjchem-1358	133	62	99.60	99.60	NUM
eurjchem-1358	133	63	s.d	s.d	PROPN
eurjchem-1358	133	64	.	.	PROPN
eurjchem-1358	134	1	0.37	0.37	NUM
eurjchem-1358	134	2	0.34	0.34	NUM
eurjchem-1358	134	3	0.73	0.73	NUM
eurjchem-1358	134	4	0.24	0.24	NUM
eurjchem-1358	134	5	0.43	0.43	NUM
eurjchem-1358	134	6	0.53	0.53	NUM
eurjchem-1358	134	7	%	%	NOUN
eurjchem-1358	134	8	r.s.d	r.s.d	NOUN
eurjchem-1358	134	9	.	.	PUNCT
eurjchem-1358	135	1	0.91	0.91	NUM
eurjchem-1358	135	2	0.67	0.67	NUM
eurjchem-1358	135	3	1.21	1.21	NUM
eurjchem-1358	135	4	0.58	0.58	NUM
eurjchem-1358	135	5	0.85	0.85	NUM
eurjchem-1358	135	6	0.89	0.89	NUM
eurjchem-1358	135	7	table	table	NOUN
eurjchem-1358	135	8	6	6	NUM
eurjchem-1358	135	9	.	.	PUNCT
eurjchem-1358	135	10	results	result	NOUN
eurjchem-1358	135	11	for	for	ADP
eurjchem-1358	135	12	determination	determination	NOUN
eurjchem-1358	135	13	of	of	ADP
eurjchem-1358	135	14	inter‐day	inter‐day	NOUN
eurjchem-1358	135	15	assay	assay	VERB
eurjchem-1358	135	16	for	for	ADP
eurjchem-1358	135	17	paba	paba	NOUN
eurjchem-1358	135	18	in	in	ADP
eurjchem-1358	135	19	bulk	bulk	ADJ
eurjchem-1358	135	20	powder	powder	NOUN
eurjchem-1358	135	21	and	and	CCONJ
eurjchem-1358	135	22	in	in	ADP
eurjchem-1358	135	23	presence	presence	NOUN
eurjchem-1358	135	24	of	of	ADP
eurjchem-1358	135	25	ob	ob	NUM
eurjchem-1358	135	26	by	by	ADP
eurjchem-1358	135	27	proposed	propose	VERB
eurjchem-1358	135	28	lc	lc	PROPN
eurjchem-1358	135	29	method	method	NOUN
eurjchem-1358	135	30	.	.	PUNCT
eurjchem-1358	136	1	sample	sample	NOUN
eurjchem-1358	136	2	inter‐day	inter‐day	PROPN
eurjchem-1358	136	3	assay	assay	VERB
eurjchem-1358	136	4	for	for	ADP
eurjchem-1358	136	5	paba	paba	NOUN
eurjchem-1358	136	6	in	in	ADP
eurjchem-1358	136	7	bulk	bulk	ADJ
eurjchem-1358	136	8	powder	powder	NOUN
eurjchem-1358	136	9	inter‐day	inter‐day	NOUN
eurjchem-1358	136	10	assay	assay	VERB
eurjchem-1358	136	11	for	for	ADP
eurjchem-1358	136	12	paba	paba	NOUN
eurjchem-1358	136	13	in	in	ADP
eurjchem-1358	136	14	presence	presence	NOUN
eurjchem-1358	136	15	of	of	ADP
eurjchem-1358	136	16	ob	ob	ADP
eurjchem-1358	136	17	concentration	concentration	NOUN
eurjchem-1358	136	18	20	20	NUM
eurjchem-1358	136	19	μg	μg	NOUN
eurjchem-1358	136	20	/	/	SYM
eurjchem-1358	136	21	ml	ml	NOUN
eurjchem-1358	136	22	80	80	NUM
eurjchem-1358	136	23	%	%	NOUN
eurjchem-1358	136	24	25	25	NUM
eurjchem-1358	136	25	μg	μg	NOUN
eurjchem-1358	136	26	/	/	SYM
eurjchem-1358	136	27	ml	ml	NOUN
eurjchem-1358	136	28	100	100	NUM
eurjchem-1358	136	29	%	%	NOUN
eurjchem-1358	136	30	30	30	NUM
eurjchem-1358	136	31	μg	μg	NOUN
eurjchem-1358	136	32	/	/	SYM
eurjchem-1358	137	1	ml	ml	NOUN
eurjchem-1358	137	2	120	120	NUM
eurjchem-1358	137	3	%	%	NOUN
eurjchem-1358	137	4	20	20	NUM
eurjchem-1358	137	5	μg	μg	NOUN
eurjchem-1358	137	6	/	/	SYM
eurjchem-1358	137	7	ml	ml	NOUN
eurjchem-1358	137	8	80	80	NUM
eurjchem-1358	137	9	%	%	NOUN
eurjchem-1358	137	10	25	25	NUM
eurjchem-1358	137	11	μg	μg	NOUN
eurjchem-1358	137	12	/	/	SYM
eurjchem-1358	137	13	ml	ml	NOUN
eurjchem-1358	137	14	100	100	NUM
eurjchem-1358	137	15	%	%	NOUN
eurjchem-1358	137	16	30	30	NUM
eurjchem-1358	137	17	μg	μg	NOUN
eurjchem-1358	137	18	/	/	SYM
eurjchem-1358	137	19	ml	ml	NOUN
eurjchem-1358	137	20	120	120	NUM
eurjchem-1358	137	21	%	%	NOUN
eurjchem-1358	137	22	mean	mean	NOUN
eurjchem-1358	137	23	19.89	19.89	NUM
eurjchem-1358	137	24	24.96	24.96	NUM
eurjchem-1358	137	25	29.92	29.92	NUM
eurjchem-1358	137	26	20.04	20.04	NUM
eurjchem-1358	137	27	24.99	24.99	NUM
eurjchem-1358	137	28	29.86	29.86	NUM
eurjchem-1358	137	29	%	%	NOUN
eurjchem-1358	137	30	recovery	recovery	NOUN
eurjchem-1358	137	31	99.45	99.45	NUM
eurjchem-1358	137	32	99.84	99.84	NUM
eurjchem-1358	137	33	99.73	99.73	NUM
eurjchem-1358	137	34	100.2	100.2	NUM
eurjchem-1358	137	35	99.96	99.96	NUM
eurjchem-1358	137	36	99.53	99.53	NUM
eurjchem-1358	137	37	s.d	s.d	PROPN
eurjchem-1358	137	38	.	.	PROPN
eurjchem-1358	137	39	0.13	0.13	NUM
eurjchem-1358	137	40	0.20	0.20	NUM
eurjchem-1358	137	41	0.38	0.38	NUM
eurjchem-1358	137	42	0.20	0.20	NUM
eurjchem-1358	137	43	0.21	0.21	NUM
eurjchem-1358	137	44	0.41	0.41	NUM
eurjchem-1358	137	45	%	%	NOUN
eurjchem-1358	137	46	r.s.d	r.s.d	ADP
eurjchem-1358	137	47	0.65	0.65	NUM
eurjchem-1358	137	48	0.82	0.82	NUM
eurjchem-1358	137	49	1.26	1.26	NUM
eurjchem-1358	137	50	0.99	0.99	NUM
eurjchem-1358	137	51	0.83	0.83	NUM
eurjchem-1358	137	52	1.38	1.38	NUM
eurjchem-1358	137	53	table	table	NOUN
eurjchem-1358	137	54	7	7	NUM
eurjchem-1358	137	55	.	.	PUNCT
eurjchem-1358	138	1	influence	influence	NOUN
eurjchem-1358	138	2	of	of	ADP
eurjchem-1358	138	3	mobile	mobile	ADJ
eurjchem-1358	138	4	phase	phase	NOUN
eurjchem-1358	138	5	flow	flow	NOUN
eurjchem-1358	138	6	rate	rate	NOUN
eurjchem-1358	138	7	on	on	ADP
eurjchem-1358	138	8	resolution	resolution	NOUN
eurjchem-1358	138	9	of	of	ADP
eurjchem-1358	138	10	ob	ob	NOUN
eurjchem-1358	138	11	in	in	ADP
eurjchem-1358	138	12	presence	presence	NOUN
eurjchem-1358	138	13	of	of	ADP
eurjchem-1358	138	14	paba	paba	PROPN
eurjchem-1358	138	15	.	.	PUNCT
eurjchem-1358	139	1	0.9	0.9	NUM
eurjchem-1358	139	2	ml	ml	NOUN
eurjchem-1358	139	3	/	/	SYM
eurjchem-1358	139	4	min	min	PROPN
eurjchem-1358	139	5	0.8	0.8	NUM
eurjchem-1358	139	6	ml	ml	NOUN
eurjchem-1358	139	7	/	/	SYM
eurjchem-1358	139	8	min0.7	min0.7	PROPN
eurjchem-1358	139	9	ml	ml	VERB
eurjchem-1358	139	10	/	/	SYM
eurjchem-1358	139	11	minflow	minflow	NOUN
eurjchem-1358	139	12	rate	rate	NOUN
eurjchem-1358	139	13	14.08	14.08	NUM
eurjchem-1358	139	14	14.6314.81	14.6314.81	NUM
eurjchem-1358	139	15	r	r	NOUN
eurjchem-1358	139	16	,	,	PUNCT
eurjchem-1358	139	17	resolution	resolution	NOUN
eurjchem-1358	139	18	factor	factor	NOUN
eurjchem-1358	139	19	table	table	NOUN
eurjchem-1358	139	20	8	8	NUM
eurjchem-1358	139	21	.	.	PUNCT
eurjchem-1358	140	1	influence	influence	NOUN
eurjchem-1358	140	2	of	of	ADP
eurjchem-1358	140	3	acetonitrile	acetonitrile	ADJ
eurjchem-1358	140	4	strength	strength	NOUN
eurjchem-1358	140	5	of	of	ADP
eurjchem-1358	140	6	mobile	mobile	ADJ
eurjchem-1358	140	7	phase	phase	NOUN
eurjchem-1358	140	8	on	on	ADP
eurjchem-1358	140	9	resolution	resolution	NOUN
eurjchem-1358	140	10	of	of	ADP
eurjchem-1358	140	11	ob	ob	NOUN
eurjchem-1358	140	12	from	from	ADP
eurjchem-1358	140	13	paba	paba	PROPN
eurjchem-1358	140	14	.	.	PUNCT
eurjchem-1358	141	1	%	%	NOUN
eurjchem-1358	141	2	of	of	ADP
eurjchem-1358	141	3	acetonitrile	acetonitrile	NOUN
eurjchem-1358	141	4	68	68	NUM
eurjchem-1358	141	5	%	%	NOUN
eurjchem-1358	141	6	70	70	NUM
eurjchem-1358	141	7	%	%	NOUN
eurjchem-1358	141	8	72	72	NUM
eurjchem-1358	141	9	%	%	NOUN
eurjchem-1358	141	10	r	r	NOUN
eurjchem-1358	141	11	,	,	PUNCT
eurjchem-1358	141	12	resolution	resolution	NOUN
eurjchem-1358	141	13	factor	factor	NOUN
eurjchem-1358	141	14	14.25	14.25	NUM
eurjchem-1358	141	15	14.63	14.63	NUM
eurjchem-1358	141	16	14.24	14.24	NUM
eurjchem-1358	141	17	table	table	NOUN
eurjchem-1358	141	18	9	9	NUM
eurjchem-1358	141	19	.	.	PUNCT
eurjchem-1358	142	1	influence	influence	NOUN
eurjchem-1358	142	2	of	of	ADP
eurjchem-1358	142	3	change	change	NOUN
eurjchem-1358	142	4	of	of	ADP
eurjchem-1358	142	5	ph	ph	NOUN
eurjchem-1358	142	6	of	of	ADP
eurjchem-1358	142	7	mobile	mobile	ADJ
eurjchem-1358	142	8	phase	phase	NOUN
eurjchem-1358	142	9	on	on	ADP
eurjchem-1358	142	10	resolution	resolution	NOUN
eurjchem-1358	142	11	of	of	ADP
eurjchem-1358	142	12	ob	ob	PROPN
eurjchem-1358	142	13	.	.	PROPN
eurjchem-1358	142	14	ph	ph	PROPN
eurjchem-1358	142	15	2.25	2.25	NUM
eurjchem-1358	142	16	2.35	2.35	NUM
eurjchem-1358	142	17	2.45	2.45	NUM
eurjchem-1358	142	18	r	r	NOUN
eurjchem-1358	142	19	,	,	PUNCT
eurjchem-1358	142	20	resolution	resolution	NOUN
eurjchem-1358	142	21	factor	factor	NOUN
eurjchem-1358	142	22	14.45	14.45	NUM
eurjchem-1358	142	23	14.63	14.63	NUM
eurjchem-1358	142	24	14.66	14.66	NUM
eurjchem-1358	142	25	the	the	DET
eurjchem-1358	142	26	values	value	NOUN
eurjchem-1358	142	27	of	of	ADP
eurjchem-1358	142	28	precision	precision	NOUN
eurjchem-1358	142	29	(	(	PUNCT
eurjchem-1358	142	30	%	%	INTJ
eurjchem-1358	142	31	r.s.d	r.s.d	NOUN
eurjchem-1358	142	32	.	.	PUNCT
eurjchem-1358	142	33	)	)	PUNCT
eurjchem-1358	142	34	of	of	ADP
eurjchem-1358	142	35	repeatability	repeatability	NOUN
eurjchem-1358	142	36	for	for	ADP
eurjchem-1358	142	37	both	both	PRON
eurjchem-1358	142	38	ob	ob	NOUN
eurjchem-1358	142	39	and	and	CCONJ
eurjchem-1358	142	40	paba	paba	NOUN
eurjchem-1358	142	41	were	be	AUX
eurjchem-1358	142	42	found	find	VERB
eurjchem-1358	142	43	to	to	PART
eurjchem-1358	142	44	be	be	AUX
eurjchem-1358	142	45	less	less	ADJ
eurjchem-1358	142	46	than	than	ADP
eurjchem-1358	142	47	1	1	NUM
eurjchem-1358	142	48	%	%	NOUN
eurjchem-1358	142	49	in	in	ADP
eurjchem-1358	142	50	the	the	DET
eurjchem-1358	142	51	three	three	NUM
eurjchem-1358	142	52	concentrations	concentration	NOUN
eurjchem-1358	142	53	,	,	PUNCT
eurjchem-1358	142	54	(	(	PUNCT
eurjchem-1358	142	55	table	table	NOUN
eurjchem-1358	142	56	3	3	NUM
eurjchem-1358	142	57	and	and	CCONJ
eurjchem-1358	142	58	4	4	NUM
eurjchem-1358	142	59	)	)	PUNCT
eurjchem-1358	142	60	.	.	PUNCT
eurjchem-1358	143	1	inter‐day	inter‐day	PROPN
eurjchem-1358	143	2	precision	precision	NOUN
eurjchem-1358	143	3	was	be	AUX
eurjchem-1358	143	4	evaluated	evaluate	VERB
eurjchem-1358	143	5	through	through	ADP
eurjchem-1358	143	6	replicate	replicate	VERB
eurjchem-1358	143	7	analysis	analysis	NOUN
eurjchem-1358	143	8	of	of	ADP
eurjchem-1358	143	9	40	40	NUM
eurjchem-1358	143	10	,	,	PUNCT
eurjchem-1358	143	11	50	50	NUM
eurjchem-1358	143	12	and	and	CCONJ
eurjchem-1358	143	13	60	60	NUM
eurjchem-1358	143	14	µg	µg	ADV
eurjchem-1358	143	15	/	/	SYM
eurjchem-1358	143	16	ml	ml	NOUN
eurjchem-1358	143	17	and	and	CCONJ
eurjchem-1358	143	18	20	20	NUM
eurjchem-1358	143	19	,	,	PUNCT
eurjchem-1358	143	20	25	25	NUM
eurjchem-1358	143	21	and	and	CCONJ
eurjchem-1358	143	22	30	30	NUM
eurjchem-1358	143	23	µg	µg	NOUN
eurjchem-1358	143	24	/	/	SYM
eurjchem-1358	143	25	ml	ml	NOUN
eurjchem-1358	143	26	for	for	ADP
eurjchem-1358	143	27	ob	ob	NOUN
eurjchem-1358	143	28	and	and	CCONJ
eurjchem-1358	143	29	paba	paba	NOUN
eurjchem-1358	143	30	for	for	ADP
eurjchem-1358	143	31	three	three	NUM
eurjchem-1358	143	32	successive	successive	ADJ
eurjchem-1358	143	33	days	day	NOUN
eurjchem-1358	143	34	.	.	PUNCT
eurjchem-1358	144	1	the	the	DET
eurjchem-1358	144	2	values	value	NOUN
eurjchem-1358	144	3	of	of	ADP
eurjchem-1358	144	4	precision	precision	NOUN
eurjchem-1358	144	5	(	(	PUNCT
eurjchem-1358	144	6	%	%	INTJ
eurjchem-1358	144	7	r.s.d	r.s.d	NOUN
eurjchem-1358	144	8	.	.	PUNCT
eurjchem-1358	144	9	)	)	PUNCT
eurjchem-1358	145	1	for	for	ADP
eurjchem-1358	145	2	ob	ob	PRON
eurjchem-1358	145	3	and	and	CCONJ
eurjchem-1358	145	4	paba	paba	NOUN
eurjchem-1358	145	5	were	be	AUX
eurjchem-1358	145	6	found	find	VERB
eurjchem-1358	145	7	to	to	PART
eurjchem-1358	145	8	be	be	AUX
eurjchem-1358	145	9	less	less	ADJ
eurjchem-1358	145	10	than	than	ADP
eurjchem-1358	145	11	2	2	NUM
eurjchem-1358	145	12	%	%	NOUN
eurjchem-1358	145	13	(	(	PUNCT
eurjchem-1358	145	14	table	table	NOUN
eurjchem-1358	145	15	5	5	NUM
eurjchem-1358	145	16	and	and	CCONJ
eurjchem-1358	145	17	6	6	NUM
eurjchem-1358	145	18	)	)	PUNCT
eurjchem-1358	145	19	.	.	PUNCT
eurjchem-1358	146	1	3.3.4	3.3.4	X
eurjchem-1358	146	2	.	.	PUNCT
eurjchem-1358	147	1	selectivity	selectivity	NOUN
eurjchem-1358	147	2	selectivity	selectivity	NOUN
eurjchem-1358	147	3	is	be	AUX
eurjchem-1358	147	4	the	the	DET
eurjchem-1358	147	5	ability	ability	NOUN
eurjchem-1358	147	6	of	of	ADP
eurjchem-1358	147	7	the	the	DET
eurjchem-1358	147	8	analytical	analytical	ADJ
eurjchem-1358	147	9	method	method	NOUN
eurjchem-1358	147	10	to	to	PART
eurjchem-1358	147	11	measure	measure	VERB
eurjchem-1358	147	12	the	the	DET
eurjchem-1358	147	13	analytes	analyte	NOUN
eurjchem-1358	147	14	in	in	ADP
eurjchem-1358	147	15	the	the	DET
eurjchem-1358	147	16	presence	presence	NOUN
eurjchem-1358	147	17	of	of	ADP
eurjchem-1358	147	18	interferences	interference	NOUN
eurjchem-1358	147	19	including	include	VERB
eurjchem-1358	147	20	degradation	degradation	NOUN
eurjchem-1358	147	21	products	product	NOUN
eurjchem-1358	147	22	or	or	CCONJ
eurjchem-1358	147	23	impurities	impurity	NOUN
eurjchem-1358	147	24	,	,	PUNCT
eurjchem-1358	147	25	related	related	ADJ
eurjchem-1358	147	26	substance	substance	NOUN
eurjchem-1358	147	27	and	and	CCONJ
eurjchem-1358	147	28	matrix	matrix	NOUN
eurjchem-1358	147	29	components	component	NOUN
eurjchem-1358	147	30	.	.	PUNCT
eurjchem-1358	148	1	in	in	ADP
eurjchem-1358	148	2	the	the	DET
eurjchem-1358	148	3	present	present	ADJ
eurjchem-1358	148	4	work	work	NOUN
eurjchem-1358	148	5	,	,	PUNCT
eurjchem-1358	148	6	ob	ob	ADP
eurjchem-1358	148	7	was	be	AUX
eurjchem-1358	148	8	determined	determine	VERB
eurjchem-1358	148	9	and	and	CCONJ
eurjchem-1358	148	10	no	no	DET
eurjchem-1358	148	11	chromatographic	chromatographic	ADJ
eurjchem-1358	148	12	interference	interference	NOUN
eurjchem-1358	148	13	from	from	ADP
eurjchem-1358	148	14	any	any	DET
eurjchem-1358	148	15	degradation	degradation	NOUN
eurjchem-1358	148	16	products	product	NOUN
eurjchem-1358	148	17	or	or	CCONJ
eurjchem-1358	148	18	excipients	excipient	NOUN
eurjchem-1358	148	19	was	be	AUX
eurjchem-1358	148	20	found	find	VERB
eurjchem-1358	148	21	at	at	ADP
eurjchem-1358	148	22	the	the	DET
eurjchem-1358	148	23	retention	retention	NOUN
eurjchem-1358	148	24	time	time	NOUN
eurjchem-1358	148	25	of	of	ADP
eurjchem-1358	148	26	examined	examine	VERB
eurjchem-1358	148	27	drug	drug	NOUN
eurjchem-1358	148	28	(	(	PUNCT
eurjchem-1358	148	29	figure	figure	NOUN
eurjchem-1358	148	30	3	3	NUM
eurjchem-1358	148	31	)	)	PUNCT
eurjchem-1358	148	32	.	.	PUNCT
eurjchem-1358	149	1	in	in	ADP
eurjchem-1358	149	2	addition	addition	NOUN
eurjchem-1358	149	3	,	,	PUNCT
eurjchem-1358	149	4	the	the	DET
eurjchem-1358	149	5	chromatogram	chromatogram	NOUN
eurjchem-1358	149	6	of	of	ADP
eurjchem-1358	149	7	the	the	DET
eurjchem-1358	149	8	sample	sample	NOUN
eurjchem-1358	149	9	solution	solution	NOUN
eurjchem-1358	149	10	was	be	AUX
eurjchem-1358	149	11	found	find	VERB
eurjchem-1358	149	12	identical	identical	ADJ
eurjchem-1358	149	13	to	to	ADP
eurjchem-1358	149	14	the	the	DET
eurjchem-1358	149	15	chromatogram	chromatogram	NOUN
eurjchem-1358	149	16	received	receive	VERB
eurjchem-1358	149	17	by	by	ADP
eurjchem-1358	149	18	ob	ob	INTJ
eurjchem-1358	149	19	standard	standard	ADJ
eurjchem-1358	149	20	solution	solution	NOUN
eurjchem-1358	149	21	.	.	PUNCT
eurjchem-1358	150	1	these	these	DET
eurjchem-1358	150	2	results	result	NOUN
eurjchem-1358	150	3	demonstrate	demonstrate	VERB
eurjchem-1358	150	4	the	the	DET
eurjchem-1358	150	5	absence	absence	NOUN
eurjchem-1358	150	6	of	of	ADP
eurjchem-1358	150	7	interference	interference	NOUN
eurjchem-1358	150	8	from	from	ADP
eurjchem-1358	150	9	other	other	ADJ
eurjchem-1358	150	10	materials	material	NOUN
eurjchem-1358	150	11	in	in	ADP
eurjchem-1358	150	12	the	the	DET
eurjchem-1358	150	13	pharmaceutical	pharmaceutical	ADJ
eurjchem-1358	150	14	formulation	formulation	NOUN
eurjchem-1358	150	15	and	and	CCONJ
eurjchem-1358	150	16	therefore	therefore	ADV
eurjchem-1358	150	17	confirm	confirm	VERB
eurjchem-1358	150	18	the	the	DET
eurjchem-1358	150	19	selectivity	selectivity	NOUN
eurjchem-1358	150	20	of	of	ADP
eurjchem-1358	150	21	proposed	propose	VERB
eurjchem-1358	150	22	method	method	NOUN
eurjchem-1358	150	23	.	.	PUNCT
eurjchem-1358	151	1	3.3.5	3.3.5	X
eurjchem-1358	151	2	.	.	PUNCT
eurjchem-1358	152	1	limit	limit	NOUN
eurjchem-1358	152	2	of	of	ADP
eurjchem-1358	152	3	detection	detection	NOUN
eurjchem-1358	152	4	and	and	CCONJ
eurjchem-1358	152	5	limit	limit	NOUN
eurjchem-1358	152	6	of	of	ADP
eurjchem-1358	152	7	quantification	quantification	NOUN
eurjchem-1358	152	8	limit	limit	NOUN
eurjchem-1358	152	9	of	of	ADP
eurjchem-1358	152	10	detection	detection	NOUN
eurjchem-1358	152	11	(	(	PUNCT
eurjchem-1358	152	12	lod	lod	PROPN
eurjchem-1358	152	13	)	)	PUNCT
eurjchem-1358	152	14	and	and	CCONJ
eurjchem-1358	152	15	limit	limit	NOUN
eurjchem-1358	152	16	of	of	ADP
eurjchem-1358	152	17	quantification	quantification	NOUN
eurjchem-1358	152	18	(	(	PUNCT
eurjchem-1358	152	19	loq	loq	PROPN
eurjchem-1358	152	20	)	)	PUNCT
eurjchem-1358	152	21	were	be	AUX
eurjchem-1358	152	22	calculated	calculate	VERB
eurjchem-1358	152	23	using	use	VERB
eurjchem-1358	152	24	following	follow	VERB
eurjchem-1358	152	25	equation	equation	NOUN
eurjchem-1358	152	26	as	as	ADP
eurjchem-1358	152	27	per	per	ADP
eurjchem-1358	152	28	ich	ich	NOUN
eurjchem-1358	152	29	guidelines	guideline	NOUN
eurjchem-1358	152	30	[	[	X
eurjchem-1358	152	31	21	21	NUM
eurjchem-1358	152	32	]	]	PUNCT
eurjchem-1358	152	33	.	.	PUNCT
eurjchem-1358	153	1	lod	lod	PROPN
eurjchem-1358	153	2	=	=	PUNCT
eurjchem-1358	153	3	3.3	3.3	NUM
eurjchem-1358	153	4	×σ	×σ	NOUN
eurjchem-1358	153	5	/	/	SYM
eurjchem-1358	153	6	s	s	X
eurjchem-1358	153	7	(	(	PUNCT
eurjchem-1358	153	8	1	1	NUM
eurjchem-1358	153	9	)	)	PUNCT
eurjchem-1358	153	10	loq	loq	NOUN
eurjchem-1358	153	11	=	=	PROPN
eurjchem-1358	153	12	10	10	NUM
eurjchem-1358	153	13	×σ	×σ	NOUN
eurjchem-1358	153	14	/s	/s	PUNCT
eurjchem-1358	153	15	(	(	PUNCT
eurjchem-1358	153	16	2	2	X
eurjchem-1358	153	17	)	)	PUNCT
eurjchem-1358	153	18	where	where	SCONJ
eurjchem-1358	153	19	σ	σ	PROPN
eurjchem-1358	153	20	is	be	AUX
eurjchem-1358	153	21	the	the	DET
eurjchem-1358	153	22	standard	standard	ADJ
eurjchem-1358	153	23	deviation	deviation	NOUN
eurjchem-1358	153	24	of	of	ADP
eurjchem-1358	153	25	response	response	NOUN
eurjchem-1358	153	26	and	and	CCONJ
eurjchem-1358	153	27	s	s	NOUN
eurjchem-1358	153	28	is	be	AUX
eurjchem-1358	153	29	the	the	DET
eurjchem-1358	153	30	slope	slope	NOUN
eurjchem-1358	153	31	of	of	ADP
eurjchem-1358	153	32	the	the	DET
eurjchem-1358	153	33	calibration	calibration	NOUN
eurjchem-1358	153	34	curve	curve	NOUN
eurjchem-1358	153	35	,	,	PUNCT
eurjchem-1358	153	36	the	the	DET
eurjchem-1358	153	37	results	result	NOUN
eurjchem-1358	153	38	are	be	AUX
eurjchem-1358	153	39	shown	show	VERB
eurjchem-1358	153	40	in	in	ADP
eurjchem-1358	153	41	table	table	NOUN
eurjchem-1358	153	42	2	2	NUM
eurjchem-1358	153	43	.	.	PUNCT
eurjchem-1358	154	1	3.3.6	3.3.6	NUM
eurjchem-1358	154	2	.	.	PUNCT
eurjchem-1358	155	1	robustness	robustness	NOUN
eurjchem-1358	155	2	robustness	robustness	NOUN
eurjchem-1358	155	3	was	be	AUX
eurjchem-1358	155	4	performed	perform	VERB
eurjchem-1358	155	5	by	by	ADP
eurjchem-1358	155	6	deliberately	deliberately	ADV
eurjchem-1358	155	7	changing	change	VERB
eurjchem-1358	155	8	the	the	DET
eurjchem-1358	155	9	chromatographic	chromatographic	ADJ
eurjchem-1358	155	10	conditions	condition	NOUN
eurjchem-1358	155	11	.	.	PUNCT
eurjchem-1358	156	1	only	only	ADV
eurjchem-1358	156	2	one	one	NUM
eurjchem-1358	156	3	factor	factor	NOUN
eurjchem-1358	156	4	was	be	AUX
eurjchem-1358	156	5	changed	change	VERB
eurjchem-1358	156	6	at	at	ADP
eurjchem-1358	156	7	a	a	DET
eurjchem-1358	156	8	time	time	NOUN
eurjchem-1358	156	9	while	while	SCONJ
eurjchem-1358	156	10	the	the	DET
eurjchem-1358	156	11	other	other	ADJ
eurjchem-1358	156	12	kept	keep	VERB
eurjchem-1358	156	13	constant	constant	ADJ
eurjchem-1358	156	14	.	.	PUNCT
eurjchem-1358	157	1	the	the	DET
eurjchem-1358	157	2	factor	factor	NOUN
eurjchem-1358	157	3	measured	measure	VERB
eurjchem-1358	157	4	after	after	SCONJ
eurjchem-1358	157	5	each	each	DET
eurjchem-1358	157	6	change	change	NOUN
eurjchem-1358	157	7	was	be	AUX
eurjchem-1358	157	8	the	the	DET
eurjchem-1358	157	9	resolution	resolution	NOUN
eurjchem-1358	157	10	factor	factor	NOUN
eurjchem-1358	157	11	between	between	ADP
eurjchem-1358	157	12	the	the	DET
eurjchem-1358	157	13	two	two	NUM
eurjchem-1358	157	14	peaks	peak	NOUN
eurjchem-1358	157	15	.	.	PUNCT
eurjchem-1358	158	1	changing	change	VERB
eurjchem-1358	158	2	the	the	DET
eurjchem-1358	158	3	flow	flow	NOUN
eurjchem-1358	158	4	rate	rate	NOUN
eurjchem-1358	158	5	of	of	ADP
eurjchem-1358	158	6	mobile	mobile	ADJ
eurjchem-1358	158	7	phase	phase	NOUN
eurjchem-1358	158	8	by	by	ADP
eurjchem-1358	158	9	±0.1	±0.1	PROPN
eurjchem-1358	158	10	,	,	PUNCT
eurjchem-1358	158	11	acetonitrile	acetonitrile	ADJ
eurjchem-1358	158	12	ratio	ratio	NOUN
eurjchem-1358	158	13	by	by	ADP
eurjchem-1358	158	14	±2	±2	NOUN
eurjchem-1358	158	15	%	%	NOUN
eurjchem-1358	158	16	,	,	PUNCT
eurjchem-1358	158	17	varying	vary	VERB
eurjchem-1358	158	18	the	the	DET
eurjchem-1358	158	19	ph	ph	NOUN
eurjchem-1358	158	20	of	of	ADP
eurjchem-1358	158	21	the	the	DET
eurjchem-1358	158	22	mobile	mobile	ADJ
eurjchem-1358	158	23	phase	phase	NOUN
eurjchem-1358	158	24	by	by	ADP
eurjchem-1358	158	25	±0.1	±0.1	NOUN
eurjchem-1358	158	26	did	do	AUX
eurjchem-1358	158	27	n’t	not	PART
eurjchem-1358	158	28	have	have	VERB
eurjchem-1358	158	29	significant	significant	ADJ
eurjchem-1358	158	30	effect	effect	NOUN
eurjchem-1358	158	31	on	on	ADP
eurjchem-1358	158	32	chromatographic	chromatographic	ADJ
eurjchem-1358	158	33	resolution	resolution	NOUN
eurjchem-1358	158	34	by	by	ADP
eurjchem-1358	158	35	the	the	DET
eurjchem-1358	158	36	proposed	propose	VERB
eurjchem-1358	158	37	lc	lc	NOUN
eurjchem-1358	158	38	method	method	NOUN
eurjchem-1358	158	39	for	for	ADP
eurjchem-1358	158	40	ob	ob	NUM
eurjchem-1358	158	41	and	and	CCONJ
eurjchem-1358	158	42	its	its	PRON
eurjchem-1358	158	43	degradation	degradation	NOUN
eurjchem-1358	158	44	product	product	NOUN
eurjchem-1358	158	45	,	,	PUNCT
eurjchem-1358	158	46	indicating	indicate	VERB
eurjchem-1358	158	47	good	good	ADJ
eurjchem-1358	158	48	robustness	robustness	NOUN
eurjchem-1358	158	49	of	of	ADP
eurjchem-1358	158	50	the	the	DET
eurjchem-1358	158	51	proposed	propose	VERB
eurjchem-1358	158	52	method	method	NOUN
eurjchem-1358	158	53	as	as	SCONJ
eurjchem-1358	158	54	shown	show	VERB
eurjchem-1358	158	55	in	in	ADP
eurjchem-1358	158	56	tables	table	NOUN
eurjchem-1358	158	57	7‐9	7‐9	NOUN
eurjchem-1358	158	58	.	.	PUNCT
eurjchem-1358	159	1	el‐kerdawy	el‐kerdawy	PROPN
eurjchem-1358	159	2	et	et	PROPN
eurjchem-1358	159	3	al	al	PROPN
eurjchem-1358	159	4	.	.	PUNCT
eurjchem-1358	159	5	/	/	SYM
eurjchem-1358	159	6	european	european	PROPN
eurjchem-1358	159	7	journal	journal	PROPN
eurjchem-1358	159	8	of	of	ADP
eurjchem-1358	159	9	chemistry	chemistry	NOUN
eurjchem-1358	159	10	7	7	NUM
eurjchem-1358	159	11	(	(	PUNCT
eurjchem-1358	159	12	1	1	NUM
eurjchem-1358	159	13	)	)	PUNCT
eurjchem-1358	159	14	(	(	PUNCT
eurjchem-1358	159	15	2016	2016	NUM
eurjchem-1358	159	16	)	)	PUNCT
eurjchem-1358	159	17	97‐101	97‐101	NOUN
eurjchem-1358	159	18	101	101	NUM
eurjchem-1358	159	19	4	4	NUM
eurjchem-1358	159	20	.	.	PUNCT
eurjchem-1358	159	21	conclusion	conclusion	NOUN
eurjchem-1358	159	22	the	the	DET
eurjchem-1358	159	23	proposed	propose	VERB
eurjchem-1358	159	24	lc	lc	NOUN
eurjchem-1358	159	25	method	method	NOUN
eurjchem-1358	159	26	has	have	VERB
eurjchem-1358	159	27	the	the	DET
eurjchem-1358	159	28	advantage	advantage	NOUN
eurjchem-1358	159	29	of	of	ADP
eurjchem-1358	159	30	simplicity	simplicity	NOUN
eurjchem-1358	159	31	,	,	PUNCT
eurjchem-1358	159	32	precision	precision	NOUN
eurjchem-1358	159	33	,	,	PUNCT
eurjchem-1358	159	34	accuracy	accuracy	NOUN
eurjchem-1358	159	35	and	and	CCONJ
eurjchem-1358	159	36	convenience	convenience	NOUN
eurjchem-1358	159	37	of	of	ADP
eurjchem-1358	159	38	separation	separation	NOUN
eurjchem-1358	159	39	and	and	CCONJ
eurjchem-1358	159	40	quantification	quantification	NOUN
eurjchem-1358	159	41	of	of	ADP
eurjchem-1358	159	42	ob	ob	PRON
eurjchem-1358	159	43	alone	alone	ADJ
eurjchem-1358	159	44	or	or	CCONJ
eurjchem-1358	159	45	in	in	ADP
eurjchem-1358	159	46	the	the	DET
eurjchem-1358	159	47	presence	presence	NOUN
eurjchem-1358	159	48	of	of	ADP
eurjchem-1358	159	49	its	its	PRON
eurjchem-1358	159	50	expected	expect	VERB
eurjchem-1358	159	51	degradation	degradation	NOUN
eurjchem-1358	159	52	product	product	NOUN
eurjchem-1358	159	53	in	in	ADP
eurjchem-1358	159	54	a	a	DET
eurjchem-1358	159	55	reasonable	reasonable	ADJ
eurjchem-1358	159	56	analysis	analysis	NOUN
eurjchem-1358	159	57	time	time	NOUN
eurjchem-1358	159	58	.	.	PUNCT
eurjchem-1358	160	1	moreover	moreover	ADV
eurjchem-1358	160	2	the	the	DET
eurjchem-1358	160	3	proposed	propose	VERB
eurjchem-1358	160	4	method	method	NOUN
eurjchem-1358	160	5	is	be	AUX
eurjchem-1358	160	6	capable	capable	ADJ
eurjchem-1358	160	7	of	of	ADP
eurjchem-1358	160	8	simultaneous	simultaneous	ADJ
eurjchem-1358	160	9	deter‐	deter‐	NOUN
eurjchem-1358	160	10	mination	mination	NOUN
eurjchem-1358	160	11	ob	ob	NOUN
eurjchem-1358	160	12	and	and	CCONJ
eurjchem-1358	160	13	it	it	PRON
eurjchem-1358	160	14	’s	’	VERB
eurjchem-1358	160	15	degradant	degradant	ADJ
eurjchem-1358	160	16	in	in	ADP
eurjchem-1358	160	17	laboratory	laboratory	NOUN
eurjchem-1358	160	18	prepared	prepare	VERB
eurjchem-1358	160	19	mixture	mixture	NOUN
eurjchem-1358	160	20	and	and	CCONJ
eurjchem-1358	160	21	pharmaceutical	pharmaceutical	NOUN
eurjchem-1358	160	22	formulation	formulation	NOUN
eurjchem-1358	160	23	.	.	PUNCT
eurjchem-1358	161	1	hence	hence	ADV
eurjchem-1358	161	2	,	,	PUNCT
eurjchem-1358	161	3	the	the	DET
eurjchem-1358	161	4	proposed	propose	VERB
eurjchem-1358	161	5	lc	lc	NOUN
eurjchem-1358	161	6	method	method	NOUN
eurjchem-1358	161	7	can	can	AUX
eurjchem-1358	161	8	be	be	AUX
eurjchem-1358	161	9	used	use	VERB
eurjchem-1358	161	10	for	for	ADP
eurjchem-1358	161	11	quality	quality	NOUN
eurjchem-1358	161	12	control	control	NOUN
eurjchem-1358	161	13	of	of	ADP
eurjchem-1358	161	14	cited	cite	VERB
eurjchem-1358	161	15	drug	drug	NOUN
eurjchem-1358	161	16	.	.	PUNCT
eurjchem-1358	162	1	acknowledgement	acknowledgement	NOUN
eurjchem-1358	162	2	the	the	DET
eurjchem-1358	162	3	authors	author	NOUN
eurjchem-1358	162	4	are	be	AUX
eurjchem-1358	162	5	thankful	thankful	ADJ
eurjchem-1358	162	6	to	to	ADP
eurjchem-1358	162	7	minapharm	minapharm	PROPN
eurjchem-1358	162	8	co.	co.	PROPN
eurjchem-1358	162	9	at	at	ADP
eurjchem-1358	162	10	egypt	egypt	PROPN
eurjchem-1358	162	11	for	for	ADP
eurjchem-1358	162	12	providing	provide	VERB
eurjchem-1358	162	13	gift	gift	NOUN
eurjchem-1358	162	14	samples	sample	NOUN
eurjchem-1358	162	15	of	of	ADP
eurjchem-1358	162	16	otilonium	otilonium	NOUN
eurjchem-1358	162	17	bromide	bromide	NOUN
eurjchem-1358	162	18	.	.	PUNCT
eurjchem-1358	163	1	references	reference	NOUN
eurjchem-1358	163	2	[	[	X
eurjchem-1358	163	3	1	1	NUM
eurjchem-1358	163	4	]	]	PUNCT
eurjchem-1358	163	5	.	.	PUNCT
eurjchem-1358	164	1	poynard	poynard	PROPN
eurjchem-1358	164	2	,	,	PUNCT
eurjchem-1358	164	3	t.	t.	PROPN
eurjchem-1358	164	4	;	;	PUNCT
eurjchem-1358	164	5	regimbeau	regimbeau	PROPN
eurjchem-1358	164	6	,	,	PUNCT
eurjchem-1358	164	7	c.	c.	PROPN
eurjchem-1358	164	8	;	;	PUNCT
eurjchem-1358	164	9	benhamou	benhamou	PROPN
eurjchem-1358	164	10	,	,	PUNCT
eurjchem-1358	164	11	y.	y.	PROPN
eurjchem-1358	164	12	aliment	aliment	PROPN
eurjchem-1358	164	13	.	.	PUNCT
eurjchem-1358	165	1	pharm	pharm	NOUN
eurjchem-1358	165	2	.	.	PUNCT
eurjchem-1358	166	1	ther	ther	PROPN
eurjchem-1358	166	2	.	.	PUNCT
eurjchem-1358	167	1	2001	2001	NUM
eurjchem-1358	167	2	,	,	PUNCT
eurjchem-1358	167	3	15(3	15(3	NUM
eurjchem-1358	167	4	)	)	PUNCT
eurjchem-1358	167	5	,	,	PUNCT
eurjchem-1358	167	6	355‐361	355‐361	PROPN
eurjchem-1358	167	7	.	.	PUNCT
eurjchem-1358	168	1	[	[	X
eurjchem-1358	168	2	2	2	NUM
eurjchem-1358	168	3	]	]	PUNCT
eurjchem-1358	168	4	.	.	PUNCT
eurjchem-1358	169	1	spinelli	spinelli	PROPN
eurjchem-1358	169	2	,	,	PUNCT
eurjchem-1358	169	3	a.	a.	PROPN
eurjchem-1358	169	4	clin	clin	PROPN
eurjchem-1358	169	5	.	.	PUNCT
eurjchem-1358	170	1	drug	drug	PROPN
eurjchem-1358	170	2	invest	invest	PROPN
eurjchem-1358	170	3	.	.	PUNCT
eurjchem-1358	171	1	2007	2007	NUM
eurjchem-1358	171	2	,	,	PUNCT
eurjchem-1358	171	3	27(1	27(1	NUM
eurjchem-1358	171	4	)	)	PUNCT
eurjchem-1358	171	5	,	,	PUNCT
eurjchem-1358	171	6	15‐33	15‐33	NUM
eurjchem-1358	171	7	.	.	PUNCT
eurjchem-1358	172	1	[	[	X
eurjchem-1358	172	2	3	3	NUM
eurjchem-1358	172	3	]	]	PUNCT
eurjchem-1358	172	4	.	.	PUNCT
eurjchem-1358	173	1	lesbros‐pantoflickova	lesbros‐pantoflickova	PROPN
eurjchem-1358	173	2	,	,	PUNCT
eurjchem-1358	173	3	d.	d.	PROPN
eurjchem-1358	173	4	;	;	PUNCT
eurjchem-1358	173	5	michetti	michetti	PROPN
eurjchem-1358	173	6	,	,	PUNCT
eurjchem-1358	173	7	p.	p.	PROPN
eurjchem-1358	173	8	;	;	PUNCT
eurjchem-1358	173	9	fried	fry	VERB
eurjchem-1358	173	10	,	,	PUNCT
eurjchem-1358	173	11	m.	m.	NOUN
eurjchem-1358	173	12	;	;	PUNCT
eurjchem-1358	173	13	beglinger	beglinger	NOUN
eurjchem-1358	173	14	,	,	PUNCT
eurjchem-1358	173	15	c.	c.	PROPN
eurjchem-1358	173	16	blum	blum	PROPN
eurjchem-1358	173	17	,	,	PUNCT
eurjchem-1358	173	18	a.	a.	PROPN
eurjchem-1358	173	19	l.	l.	PROPN
eurjchem-1358	173	20	aliment	aliment	PROPN
eurjchem-1358	173	21	.	.	PUNCT
eurjchem-1358	174	1	pharm	pharm	PROPN
eurjchem-1358	174	2	.	.	PUNCT
eurjchem-1358	175	1	ther	ther	PROPN
eurjchem-1358	175	2	.	.	PUNCT
eurjchem-1358	176	1	2004	2004	NUM
eurjchem-1358	176	2	,	,	PUNCT
eurjchem-1358	176	3	20(11‐12	20(11‐12	NUM
eurjchem-1358	176	4	)	)	PUNCT
eurjchem-1358	176	5	,	,	PUNCT
eurjchem-1358	176	6	1253‐1269	1253‐1269	NUM
eurjchem-1358	176	7	.	.	PUNCT
eurjchem-1358	177	1	[	[	X
eurjchem-1358	177	2	4	4	NUM
eurjchem-1358	177	3	]	]	PUNCT
eurjchem-1358	177	4	.	.	PUNCT
eurjchem-1358	177	5	signorini	signorini	PROPN
eurjchem-1358	177	6	,	,	PUNCT
eurjchem-1358	177	7	c.	c.	NOUN
eurjchem-1358	177	8	;	;	PUNCT
eurjchem-1358	177	9	tosoni	tosoni	NOUN
eurjchem-1358	177	10	,	,	PUNCT
eurjchem-1358	177	11	s.	s.	PROPN
eurjchem-1358	177	12	;	;	PUNCT
eurjchem-1358	177	13	ballerini	ballerini	PROPN
eurjchem-1358	177	14	,	,	PUNCT
eurjchem-1358	177	15	r.	r.	PROPN
eurjchem-1358	177	16	;	;	PUNCT
eurjchem-1358	177	17	chinol	chinol	NOUN
eurjchem-1358	177	18	,	,	PUNCT
eurjchem-1358	177	19	m.	m.	NOUN
eurjchem-1358	177	20	;	;	PUNCT
eurjchem-1358	177	21	mannucci	mannucci	PROPN
eurjchem-1358	177	22	,	,	PUNCT
eurjchem-1358	177	23	c.	c.	PROPN
eurjchem-1358	177	24	drug	drug	PROPN
eurjchem-1358	177	25	.	.	PUNCT
eurjchem-1358	178	1	exp	exp	PROPN
eurjchem-1358	178	2	.	.	PUNCT
eurjchem-1358	179	1	clin	clin	PROPN
eurjchem-1358	179	2	.	.	PUNCT
eurjchem-1358	180	1	res	res	PROPN
eurjchem-1358	180	2	.	.	PROPN
eurjchem-1358	180	3	1984	1984	NUM
eurjchem-1358	180	4	,	,	PUNCT
eurjchem-1358	180	5	10	10	NUM
eurjchem-1358	180	6	,	,	PUNCT
eurjchem-1358	180	7	273‐276	273‐276	NUM
eurjchem-1358	180	8	.	.	PUNCT
eurjchem-1358	181	1	[	[	X
eurjchem-1358	181	2	5	5	NUM
eurjchem-1358	181	3	]	]	PUNCT
eurjchem-1358	181	4	.	.	PUNCT
eurjchem-1358	181	5	sutton	sutton	PROPN
eurjchem-1358	181	6	,	,	PUNCT
eurjchem-1358	181	7	j.	j.	PROPN
eurjchem-1358	181	8	a.	a.	PROPN
eurjchem-1358	181	9	;	;	PUNCT
eurjchem-1358	181	10	kilminster	kilminster	PROPN
eurjchem-1358	181	11	,	,	PUNCT
eurjchem-1358	181	12	s.	s.	PROPN
eurjchem-1358	181	13	g.	g.	PROPN
eurjchem-1358	181	14	;	;	PUNCT
eurjchem-1358	181	15	mould	mould	AUX
eurjchem-1358	181	16	,	,	PUNCT
eurjchem-1358	181	17	g.	g.	PROPN
eurjchem-1358	181	18	p.	p.	PROPN
eurjchem-1358	181	19	eur	eur	PROPN
eurjchem-1358	181	20	.	.	PUNCT
eurjchem-1358	182	1	j.	j.	PROPN
eurjchem-1358	182	2	clin	clin	PROPN
eurjchem-1358	182	3	.	.	PUNCT
eurjchem-1358	183	1	pharmacol	pharmacol	PROPN
eurjchem-1358	183	2	.	.	PUNCT
eurjchem-1358	184	1	1997	1997	NUM
eurjchem-1358	184	2	,	,	PUNCT
eurjchem-1358	184	3	52(5	52(5	NUM
eurjchem-1358	184	4	)	)	PUNCT
eurjchem-1358	184	5	,	,	PUNCT
eurjchem-1358	184	6	365‐369	365‐369	NUM
eurjchem-1358	184	7	.	.	PUNCT
eurjchem-1358	185	1	[	[	X
eurjchem-1358	185	2	6	6	NUM
eurjchem-1358	185	3	]	]	PUNCT
eurjchem-1358	185	4	.	.	PUNCT
eurjchem-1358	186	1	zhao	zhao	PROPN
eurjchem-1358	186	2	,	,	PUNCT
eurjchem-1358	186	3	y.	y.	PROPN
eurjchem-1358	186	4	r.	r.	PROPN
eurjchem-1358	186	5	;	;	PUNCT
eurjchem-1358	186	6	ding	ding	NOUN
eurjchem-1358	186	7	,	,	PUNCT
eurjchem-1358	186	8	li	li	PROPN
eurjchem-1358	186	9	;	;	PUNCT
eurjchem-1358	186	10	fan	fan	PROPN
eurjchem-1358	186	11	,	,	PUNCT
eurjchem-1358	186	12	h.	h.	PROPN
eurjchem-1358	186	13	w.	w.	PROPN
eurjchem-1358	186	14	;	;	PUNCT
eurjchem-1358	186	15	yu	yu	PROPN
eurjchem-1358	186	16	,	,	PUNCT
eurjchem-1358	186	17	y.	y.	PROPN
eurjchem-1358	186	18	;	;	PUNCT
eurjchem-1358	186	19	qi	qi	PROPN
eurjchem-1358	186	20	,	,	PUNCT
eurjchem-1358	186	21	x.	x.	NOUN
eurjchem-1358	186	22	m.	m.	NOUN
eurjchem-1358	186	23	;	;	PUNCT
eurjchem-1358	187	1	leng	leng	PROPN
eurjchem-1358	187	2	,	,	PUNCT
eurjchem-1358	187	3	y.	y.	PROPN
eurjchem-1358	187	4	;	;	PUNCT
eurjchem-1358	187	5	rao	rao	PROPN
eurjchem-1358	187	6	,	,	PUNCT
eurjchem-1358	187	7	y.	y.	PROPN
eurjchem-1358	187	8	k.	k.	PROPN
eurjchem-1358	188	1	j.	j.	PROPN
eurjchem-1358	188	2	chromatogr	chromatogr	PROPN
eurjchem-1358	188	3	.	.	PUNCT
eurjchem-1358	189	1	b	b	X
eurjchem-1358	189	2	2010	2010	NUM
eurjchem-1358	189	3	,	,	PUNCT
eurjchem-1358	189	4	878(28	878(28	NUM
eurjchem-1358	189	5	)	)	PUNCT
eurjchem-1358	189	6	,	,	PUNCT
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eurjchem-1358	190	3	]	]	PUNCT
eurjchem-1358	190	4	.	.	PUNCT
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eurjchem-1358	191	2	,	,	PUNCT
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eurjchem-1358	191	6	,	,	PUNCT
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eurjchem-1358	191	14	,	,	PUNCT
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eurjchem-1358	191	18	,	,	PUNCT
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eurjchem-1358	191	22	.	.	PUNCT
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eurjchem-1358	192	2	.	.	PUNCT
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eurjchem-1358	193	2	.	.	PUNCT
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eurjchem-1358	194	2	,	,	PUNCT
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eurjchem-1358	194	4	)	)	PUNCT
eurjchem-1358	194	5	,	,	PUNCT
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eurjchem-1358	195	3	]	]	PUNCT
eurjchem-1358	195	4	.	.	PUNCT
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eurjchem-1358	196	2	,	,	PUNCT
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eurjchem-1358	196	4	;	;	PUNCT
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eurjchem-1358	196	14	,	,	PUNCT
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eurjchem-1358	196	16	;	;	PUNCT
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eurjchem-1358	196	18	,	,	PUNCT
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eurjchem-1358	196	22	,	,	PUNCT
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eurjchem-1358	196	24	,	,	PUNCT
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eurjchem-1358	196	26	.	.	PUNCT
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eurjchem-1358	197	3	]	]	PUNCT
eurjchem-1358	197	4	.	.	PUNCT
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eurjchem-1358	197	6	,	,	PUNCT
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eurjchem-1358	197	8	;	;	PUNCT
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eurjchem-1358	197	10	,	,	PUNCT
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eurjchem-1358	197	14	,	,	PUNCT
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eurjchem-1358	197	18	,	,	PUNCT
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eurjchem-1358	197	22	,	,	PUNCT
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eurjchem-1358	197	26	,	,	PUNCT
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eurjchem-1358	197	28	j.	j.	PROPN
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eurjchem-1358	197	30	.	.	PUNCT
eurjchem-1358	198	1	sci	sci	PROPN
eurjchem-1358	198	2	.	.	PROPN
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eurjchem-1358	198	4	,	,	PUNCT
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eurjchem-1358	198	6	)	)	PUNCT
eurjchem-1358	198	7	,	,	PUNCT
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eurjchem-1358	198	9	370	370	NUM
eurjchem-1358	198	10	.	.	PUNCT
eurjchem-1358	199	1	[	[	X
eurjchem-1358	199	2	10	10	NUM
eurjchem-1358	199	3	]	]	PUNCT
eurjchem-1358	199	4	.	.	PUNCT
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eurjchem-1358	200	2	,	,	PUNCT
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eurjchem-1358	200	4	;	;	PUNCT
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eurjchem-1358	200	6	,	,	PUNCT
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eurjchem-1358	200	8	;	;	PUNCT
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eurjchem-1358	200	10	,	,	PUNCT
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eurjchem-1358	200	12	;	;	PUNCT
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eurjchem-1358	200	14	,	,	PUNCT
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eurjchem-1358	200	18	,	,	PUNCT
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eurjchem-1358	200	20	;	;	PUNCT
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eurjchem-1358	200	22	,	,	PUNCT
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eurjchem-1358	200	24	int	int	PROPN
eurjchem-1358	200	25	.	.	PUNCT
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eurjchem-1358	201	3	.	.	PUNCT
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eurjchem-1358	202	2	,	,	PUNCT
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eurjchem-1358	202	4	)	)	PUNCT
eurjchem-1358	202	5	,	,	PUNCT
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eurjchem-1358	202	7	.	.	PUNCT
eurjchem-1358	203	1	[	[	X
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eurjchem-1358	203	3	]	]	PUNCT
eurjchem-1358	203	4	.	.	PUNCT
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eurjchem-1358	203	6	,	,	PUNCT
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eurjchem-1358	203	8	;	;	PUNCT
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eurjchem-1358	203	10	,	,	PUNCT
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eurjchem-1358	203	12	;	;	PUNCT
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eurjchem-1358	203	14	,	,	PUNCT
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eurjchem-1358	203	30	,	,	PUNCT
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eurjchem-1358	203	38	,	,	PUNCT
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eurjchem-1358	203	42	,	,	PUNCT
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eurjchem-1358	203	45	,	,	PUNCT
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eurjchem-1358	203	47	.	.	PUNCT
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eurjchem-1358	204	3	]	]	PUNCT
eurjchem-1358	204	4	.	.	PUNCT
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eurjchem-1358	205	2	,	,	PUNCT
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eurjchem-1358	205	5	;	;	PUNCT
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eurjchem-1358	205	7	,	,	PUNCT
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eurjchem-1358	205	10	;	;	PUNCT
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eurjchem-1358	205	12	.	.	PUNCT
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eurjchem-1358	206	2	;	;	PUNCT
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eurjchem-1358	206	4	,	,	PUNCT
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eurjchem-1358	206	7	;	;	PUNCT
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eurjchem-1358	206	9	,	,	PUNCT
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eurjchem-1358	206	12	;	;	PUNCT
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eurjchem-1358	206	14	,	,	PUNCT
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eurjchem-1358	206	17	;	;	PUNCT
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eurjchem-1358	206	19	,	,	PUNCT
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eurjchem-1358	206	23	.	.	PUNCT
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eurjchem-1358	207	2	.	.	PUNCT
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eurjchem-1358	208	2	.	.	PROPN
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eurjchem-1358	208	4	,	,	PUNCT
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eurjchem-1358	208	7	,	,	PUNCT
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eurjchem-1358	208	9	.	.	PUNCT
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eurjchem-1358	209	3	]	]	PUNCT
eurjchem-1358	209	4	.	.	PUNCT
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eurjchem-1358	209	6	,	,	PUNCT
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eurjchem-1358	209	8	;	;	PUNCT
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eurjchem-1358	209	12	;	;	PUNCT
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eurjchem-1358	209	14	,	,	PUNCT
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eurjchem-1358	209	16	;	;	PUNCT
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eurjchem-1358	209	21	;	;	PUNCT
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eurjchem-1358	209	24	,	,	PUNCT
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eurjchem-1358	209	34	)	)	PUNCT
eurjchem-1358	209	35	,	,	PUNCT
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eurjchem-1358	209	37	.	.	PUNCT
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eurjchem-1358	210	3	]	]	SYM
eurjchem-1358	210	4	.	.	PUNCT
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eurjchem-1358	211	5	.	.	PUNCT
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eurjchem-1358	212	3	.	.	PUNCT
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eurjchem-1358	213	2	.	.	PUNCT
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eurjchem-1358	214	2	,	,	PUNCT
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eurjchem-1358	214	4	,	,	PUNCT
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eurjchem-1358	214	6	.	.	PUNCT
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eurjchem-1358	215	3	]	]	PUNCT
eurjchem-1358	215	4	.	.	PUNCT
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eurjchem-1358	216	2	,	,	PUNCT
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eurjchem-1358	216	4	;	;	PUNCT
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eurjchem-1358	216	6	,	,	PUNCT
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eurjchem-1358	216	10	,	,	PUNCT
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eurjchem-1358	216	14	,	,	PUNCT
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eurjchem-1358	216	18	,	,	PUNCT
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eurjchem-1358	216	22	,	,	PUNCT
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eurjchem-1358	216	26	.	.	PUNCT
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eurjchem-1358	217	2	.	.	PROPN
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eurjchem-1358	217	4	,	,	PUNCT
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eurjchem-1358	218	3	]	]	PUNCT
eurjchem-1358	218	4	.	.	PUNCT
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eurjchem-1358	218	6	,	,	PUNCT
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eurjchem-1358	218	9	;	;	PUNCT
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eurjchem-1358	218	17	.	.	PUNCT
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eurjchem-1358	219	2	,	,	PUNCT
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eurjchem-1358	220	3	]	]	PUNCT
eurjchem-1358	220	4	.	.	PUNCT
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eurjchem-1358	221	6	,	,	PUNCT
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eurjchem-1358	224	2	,	,	PUNCT
eurjchem-1358	224	3	368	368	NUM
eurjchem-1358	224	4	,	,	PUNCT
eurjchem-1358	224	5	534‐539	534‐539	NUM
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eurjchem-1358	225	3	]	]	PUNCT
eurjchem-1358	225	4	.	.	PUNCT
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eurjchem-1358	226	2	,	,	PUNCT
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eurjchem-1358	226	6	,	,	PUNCT
eurjchem-1358	226	7	l.	l.	PROPN
eurjchem-1358	226	8	;	;	PUNCT
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eurjchem-1358	226	10	,	,	PUNCT
eurjchem-1358	226	11	y.	y.	PROPN
eurjchem-1358	226	12	;	;	PUNCT
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eurjchem-1358	226	15	x.	x.	NOUN
eurjchem-1358	226	16	;	;	PUNCT
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eurjchem-1358	226	20	j.	j.	PROPN
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eurjchem-1358	228	2	,	,	PUNCT
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eurjchem-1358	228	4	)	)	PUNCT
eurjchem-1358	228	5	,	,	PUNCT
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eurjchem-1358	228	7	.	.	PUNCT
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eurjchem-1358	229	3	]	]	PUNCT
eurjchem-1358	229	4	.	.	PUNCT
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eurjchem-1358	231	2	:	:	PUNCT
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eurjchem-1358	231	6	action	action	NOUN
eurjchem-1358	231	7	1	1	NUM
eurjchem-1358	231	8	,	,	PUNCT
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eurjchem-1358	232	3	]	]	PUNCT
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eurjchem-1358	233	3	l.	l.	PROPN
eurjchem-1358	233	4	;	;	PUNCT
eurjchem-1358	233	5	kirkland	kirkland	PROPN
eurjchem-1358	233	6	,	,	PUNCT
eurjchem-1358	233	7	j.	j.	PROPN
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eurjchem-1358	233	10	,	,	PUNCT
eurjchem-1358	233	11	j.	j.	PROPN
eurjchem-1358	233	12	ed	ed	PROPN
eurjchem-1358	233	13	.	.	PROPN
eurjchem-1358	233	14	;	;	PUNCT
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eurjchem-1358	233	17	new	new	PROPN
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eurjchem-1358	233	19	,	,	PUNCT
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eurjchem-1358	233	23	,	,	PUNCT
eurjchem-1358	233	24	toronto	toronto	PROPN
eurjchem-1358	233	25	,	,	PUNCT
eurjchem-1358	233	26	singapore	singapore	PROPN
eurjchem-1358	233	27	,	,	PUNCT
eurjchem-1358	233	28	1988	1988	NUM
eurjchem-1358	233	29	.	.	PUNCT
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eurjchem-1358	234	2	21	21	NUM
eurjchem-1358	234	3	]	]	PUNCT
eurjchem-1358	234	4	.	.	PUNCT
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eurjchem-1358	235	3	tripartite	tripartite	ADJ
eurjchem-1358	235	4	guideline	guideline	NOUN
eurjchem-1358	235	5	,	,	PUNCT
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eurjchem-1358	235	9	procedures	procedure	NOUN
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eurjchem-1358	235	19	step	step	NOUN
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eurjchem-1358	235	22	,	,	PUNCT
eurjchem-1358	235	23	parent	parent	NOUN
eurjchem-1358	235	24	guidelines	guideline	NOUN
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eurjchem-1358	235	31	,	,	PUNCT
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eurjchem-1358	235	33	in	in	ADP
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eurjchem-1358	235	35	2005	2005	NUM
eurjchem-1358	235	36	.	.	PUNCT