id	sid	tid	token	lemma	pos
eurjchem-1369	1	1	untitled	untitled	ADJ
eurjchem-1369	1	2	issn	issn	PROPN
eurjchem-1369	1	3	215	215	NUM
eurjchem-1369	1	4	reaction	reaction	NOUN
eurjchem-1369	1	5	pyrazol	pyrazol	NOUN
eurjchem-1369	1	6	husien	husien	PROPN
eurjchem-1369	1	7	ha	ha	INTJ
eurjchem-1369	1	8	chemistry	chemistry	NOUN
eurjchem-1369	1	9	depa	depa	NOUN
eurjchem-1369	1	10	*	*	PUNCT
eurjchem-1369	1	11	corresponding	correspond	VERB
eurjchem-1369	1	12	tel	tel	PROPN
eurjchem-1369	1	13	.	.	PUNCT
eurjchem-1369	1	14	:	:	PUNCT
eurjchem-1369	2	1	+20.11.208	+20.11.208	ADJ
eurjchem-1369	2	2	article	article	NOUN
eurjchem-1369	2	3	in	in	ADP
eurjchem-1369	2	4	doi	doi	PROPN
eurjchem-1369	2	5	:	:	PUNCT
eurjchem-1369	2	6	10.5155	10.5155	NUM
eurjchem-1369	2	7	/	/	SYM
eurjchem-1369	2	8	e	e	NOUN
eurjchem-1369	2	9	received	receive	VERB
eurjchem-1369	2	10	:	:	PUNCT
eurjchem-1369	2	11	18	18	NUM
eurjchem-1369	2	12	no	no	PRON
eurjchem-1369	2	13	received	receive	VERB
eurjchem-1369	2	14	in	in	ADP
eurjchem-1369	2	15	rev	rev	PROPN
eurjchem-1369	2	16	accepted	accept	VERB
eurjchem-1369	2	17	:	:	PUNCT
eurjchem-1369	2	18	01	01	NUM
eurjchem-1369	2	19	ja	ja	PROPN
eurjchem-1369	2	20	published	publish	VERB
eurjchem-1369	2	21	onlin	onlin	PROPN
eurjchem-1369	2	22	printed	print	VERB
eurjchem-1369	2	23	:	:	PUNCT
eurjchem-1369	2	24	31	31	NUM
eurjchem-1369	2	25	mar	mar	PROPN
eurjchem-1369	2	26	keywords	keyword	NOUN
eurjchem-1369	2	27	amidines	amidine	VERB
eurjchem-1369	2	28	heterocycles	heterocycle	NOUN
eurjchem-1369	2	29	electrophiles	electrophile	NOUN
eurjchem-1369	2	30	aminopyrazole	aminopyrazole	NOUN
eurjchem-1369	2	31	pyrazolotriazin	pyrazolotriazin	NOUN
eurjchem-1369	2	32	pyrazolopyrimi	pyrazolopyrimi	PROPN
eurjchem-1369	2	33	1	1	NUM
eurjchem-1369	2	34	.	.	PUNCT
eurjchem-1369	2	35	introduct	introduct	NOUN
eurjchem-1369	2	36	aminopy	aminopy	ADP
eurjchem-1369	2	37	synthesis	synthesis	NOUN
eurjchem-1369	2	38	o	o	NOUN
eurjchem-1369	2	39	various	various	ADJ
eurjchem-1369	2	40	type	type	NOUN
eurjchem-1369	2	41	pyrazolopyri	pyrazolopyri	NOUN
eurjchem-1369	2	42	pyrimidines	pyrimidine	VERB
eurjchem-1369	2	43	perties	pertie	NOUN
eurjchem-1369	2	44	as	as	SCONJ
eurjchem-1369	2	45	pu	pu	PROPN
eurjchem-1369	2	46	compounds	compound	VERB
eurjchem-1369	2	47	interest	interest	NOUN
eurjchem-1369	2	48	beca	beca	PROPN
eurjchem-1369	2	49	somal	somal	PROPN
eurjchem-1369	2	50	activit	activit	PROPN
eurjchem-1369	2	51	antagonist	antagonist	NOUN
eurjchem-1369	2	52	[	[	PUNCT
eurjchem-1369	2	53	selective	selective	ADJ
eurjchem-1369	2	54	inh	inh	NOUN
eurjchem-1369	3	1	[	[	X
eurjchem-1369	3	2	14	14	NUM
eurjchem-1369	3	3	]	]	PUNCT
eurjchem-1369	3	4	and	and	CCONJ
eurjchem-1369	3	5	as	as	ADP
eurjchem-1369	3	6	k	k	PRON
eurjchem-1369	3	7	n‐bis(me	n‐bis(me	VERB
eurjchem-1369	4	1	extremely	extremely	ADV
eurjchem-1369	4	2	i	i	PRON
eurjchem-1369	4	3	duction	duction	NOUN
eurjchem-1369	4	4	of	of	ADP
eurjchem-1369	4	5	n	n	CCONJ
eurjchem-1369	4	6	active	active	ADJ
eurjchem-1369	4	7	methy	methy	NOUN
eurjchem-1369	4	8	synthesis	synthesis	NOUN
eurjchem-1369	4	9	of	of	ADP
eurjchem-1369	4	10	study	study	NOUN
eurjchem-1369	4	11	was	be	AUX
eurjchem-1369	4	12	t	t	NOUN
eurjchem-1369	4	13	reagents	reagent	NOUN
eurjchem-1369	4	14	on	on	ADP
eurjchem-1369	4	15	ethyl	ethyl	PROPN
eurjchem-1369	4	16	ester	ester	NOUN
eurjchem-1369	4	17	(	(	PUNCT
eurjchem-1369	4	18	and	and	CCONJ
eurjchem-1369	4	19	pyrazolo	pyrazolo	ADJ
eurjchem-1369	4	20	53‐2249	53‐2249	NUM
eurjchem-1369	4	21	(	(	PUNCT
eurjchem-1369	4	22	print	print	NOUN
eurjchem-1369	4	23	)	)	PUNCT
eurjchem-1369	4	24	ns	n	VERB
eurjchem-1369	4	25	with	with	ADP
eurjchem-1369	4	26	h	h	NOUN
eurjchem-1369	4	27	o[1,5‐a]p	o[1,5‐a]p	ADJ
eurjchem-1369	4	28	asan	asan	ADJ
eurjchem-1369	4	29	abbas‐	abbas‐	NOUN
eurjchem-1369	4	30	artment	artment	NOUN
eurjchem-1369	4	31	,	,	PUNCT
eurjchem-1369	4	32	faculty	faculty	NOUN
eurjchem-1369	4	33	of	of	ADP
eurjchem-1369	4	34	g	g	PROPN
eurjchem-1369	4	35	author	author	NOUN
eurjchem-1369	4	36	at	at	ADP
eurjchem-1369	4	37	:	:	PUNCT
eurjchem-1369	4	38	chemis	chemis	PROPN
eurjchem-1369	4	39	887165	887165	NUM
eurjchem-1369	4	40	.	.	PUNCT
eurjchem-1369	5	1	fax	fax	NOUN
eurjchem-1369	5	2	:	:	PUNCT
eurjchem-1369	5	3	+20.96	+20.96	ADJ
eurjchem-1369	5	4	formation	formation	NOUN
eurjchem-1369	5	5	eurjchem.7.1.107‐1	eurjchem.7.1.107‐1	PUNCT
eurjchem-1369	5	6	ovember	ovember	NOUN
eurjchem-1369	5	7	2015	2015	NUM
eurjchem-1369	5	8	vised	vise	VERB
eurjchem-1369	5	9	form	form	NOUN
eurjchem-1369	5	10	:	:	PUNCT
eurjchem-1369	5	11	27	27	NUM
eurjchem-1369	5	12	dece	dece	PROPN
eurjchem-1369	5	13	anuary	anuary	PROPN
eurjchem-1369	5	14	2016	2016	NUM
eurjchem-1369	5	15	ne	ne	PROPN
eurjchem-1369	5	16	:	:	PUNCT
eurjchem-1369	5	17	31	31	NUM
eurjchem-1369	5	18	march	march	PROPN
eurjchem-1369	5	19	2016	2016	NUM
eurjchem-1369	5	20	rch	rch	NOUN
eurjchem-1369	5	21	2016	2016	NUM
eurjchem-1369	5	22	s	s	PART
eurjchem-1369	5	23	es	es	X
eurjchem-1369	5	24	nes	nes	PROPN
eurjchem-1369	5	25	idines	idine	NOUN
eurjchem-1369	5	26	tion	tion	PROPN
eurjchem-1369	5	27	yrazoles	yrazoles	PROPN
eurjchem-1369	5	28	are	be	AUX
eurjchem-1369	5	29	f	f	PROPN
eurjchem-1369	5	30	biologically	biologically	ADV
eurjchem-1369	5	31	es	es	X
eurjchem-1369	5	32	of	of	ADP
eurjchem-1369	5	33	biological	biological	ADJ
eurjchem-1369	5	34	imidines	imidine	NOUN
eurjchem-1369	5	35	and	and	CCONJ
eurjchem-1369	5	36	[	[	X
eurjchem-1369	5	37	1,2	1,2	NUM
eurjchem-1369	5	38	]	]	PUNCT
eurjchem-1369	5	39	are	be	AUX
eurjchem-1369	5	40	purin	purin	NOUN
eurjchem-1369	5	41	urine	urine	NOUN
eurjchem-1369	5	42	antimetab	antimetab	NOUN
eurjchem-1369	5	43	of	of	ADP
eurjchem-1369	5	44	this	this	DET
eurjchem-1369	5	45	class	class	NOUN
eurjchem-1369	5	46	ha	ha	INTJ
eurjchem-1369	5	47	ause	ause	PROPN
eurjchem-1369	5	48	of	of	ADP
eurjchem-1369	5	49	their	their	PRON
eurjchem-1369	5	50	a	a	DET
eurjchem-1369	5	51	ty	ty	NOUN
eurjchem-1369	6	1	[	[	X
eurjchem-1369	6	2	6	6	NUM
eurjchem-1369	6	3	]	]	PUNCT
eurjchem-1369	6	4	,	,	PUNCT
eurjchem-1369	6	5	antibacte	antibacte	NOUN
eurjchem-1369	7	1	[	[	X
eurjchem-1369	7	2	11	11	NUM
eurjchem-1369	7	3	]	]	PUNCT
eurjchem-1369	7	4	,	,	PUNCT
eurjchem-1369	7	5	hmg‐coa	hmg‐coa	PROPN
eurjchem-1369	7	6	hibitors	hibitor	NOUN
eurjchem-1369	7	7	[	[	X
eurjchem-1369	7	8	13	13	NUM
eurjchem-1369	7	9	]	]	PUNCT
eurjchem-1369	7	10	,	,	PUNCT
eurjchem-1369	7	11	a	a	DET
eurjchem-1369	7	12	kdr	kdr	PROPN
eurjchem-1369	7	13	kinase	kinase	PROPN
eurjchem-1369	7	14	inhi	inhi	PROPN
eurjchem-1369	7	15	ethylthio)methy	ethylthio)methy	PROPN
eurjchem-1369	7	16	nteresting	nteresting	NOUN
eurjchem-1369	7	17	ele	ele	PROPN
eurjchem-1369	7	18	ot	ot	VERB
eurjchem-1369	7	19	only	only	ADV
eurjchem-1369	7	20	an	an	DET
eurjchem-1369	7	21	ami	ami	NOUN
eurjchem-1369	7	22	ylene	ylene	PROPN
eurjchem-1369	7	23	compoun	compoun	PROPN
eurjchem-1369	7	24	heterocyclic	heterocyclic	PROPN
eurjchem-1369	7	25	co	co	VERB
eurjchem-1369	7	26	to	to	PART
eurjchem-1369	7	27	investigate	investigate	VERB
eurjchem-1369	7	28	t	t	PROPN
eurjchem-1369	7	29	5‐amino‐3‐ure	5‐amino‐3‐ure	NUM
eurjchem-1369	7	30	(	(	PUNCT
eurjchem-1369	7	31	4a	4a	NUM
eurjchem-1369	7	32	)	)	PUNCT
eurjchem-1369	7	33	in	in	ADP
eurjchem-1369	7	34	the	the	DET
eurjchem-1369	7	35	syn	syn	PROPN
eurjchem-1369	7	36	otriazine	otriazine	ADJ
eurjchem-1369	7	37	deriva	deriva	NOUN
eurjchem-1369	7	38	e	e	PROPN
eurjchem-1369	7	39	/	/	SYM
eurjchem-1369	7	40	issn	issn	PROPN
eurjchem-1369	7	41	2153‐225	2153‐225	NUM
eurjchem-1369	7	42	htt	htt	NOUN
eurjchem-1369	7	43	europ	europ	PROPN
eurjchem-1369	7	44	eterocycl	eterocycl	PROPN
eurjchem-1369	7	45	pyrimidine	pyrimidine	PROPN
eurjchem-1369	7	46	temirek	temirek	PROPN
eurjchem-1369	7	47	an	an	DET
eurjchem-1369	7	48	science	science	NOUN
eurjchem-1369	7	49	,	,	PUNCT
eurjchem-1369	7	50	south	south	PROPN
eurjchem-1369	7	51	vall	vall	PROPN
eurjchem-1369	7	52	stry	stry	PROPN
eurjchem-1369	7	53	department	department	PROPN
eurjchem-1369	7	54	,	,	PUNCT
eurjchem-1369	7	55	fa	fa	PROPN
eurjchem-1369	7	56	6.5211279	6.5211279	NUM
eurjchem-1369	7	57	.	.	PUNCT
eurjchem-1369	7	58	e‐mail	e‐mail	PUNCT
eurjchem-1369	8	1	a	a	DET
eurjchem-1369	8	2	114.1369	114.1369	PROPN
eurjchem-1369	8	3	ember	ember	NOUN
eurjchem-1369	8	4	2015	2015	NUM
eurjchem-1369	8	5	versatile	versatile	ADJ
eurjchem-1369	8	6	inte	inte	NOUN
eurjchem-1369	8	7	interesting	interesting	ADJ
eurjchem-1369	8	8	p	p	NOUN
eurjchem-1369	8	9	activity	activity	NOUN
eurjchem-1369	8	10	have	have	VERB
eurjchem-1369	8	11	pyrazolotriazin	pyrazolotriazin	NOUN
eurjchem-1369	8	12	ne	ne	PROPN
eurjchem-1369	8	13	analogues	analogue	NOUN
eurjchem-1369	8	14	a	a	DET
eurjchem-1369	8	15	bolites	bolite	NOUN
eurjchem-1369	8	16	[	[	X
eurjchem-1369	8	17	3	3	X
eurjchem-1369	8	18	]	]	PUNCT
eurjchem-1369	8	19	in	in	ADP
eurjchem-1369	8	20	bi	bi	PROPN
eurjchem-1369	8	21	ave	ave	PROPN
eurjchem-1369	8	22	attracted	attract	VERB
eurjchem-1369	8	23	a	a	DET
eurjchem-1369	8	24	w	w	NOUN
eurjchem-1369	8	25	antitrypanosom	antitrypanosom	NOUN
eurjchem-1369	8	26	erial	erial	ADJ
eurjchem-1369	9	1	[	[	X
eurjchem-1369	9	2	7,8	7,8	NUM
eurjchem-1369	9	3	]	]	PUNCT
eurjchem-1369	9	4	,	,	PUNCT
eurjchem-1369	9	5	anti‐	anti‐	PROPN
eurjchem-1369	9	6	a	a	DET
eurjchem-1369	9	7	reductase	reductase	NOUN
eurjchem-1369	9	8	inh	inh	PROPN
eurjchem-1369	9	9	amp	amp	PROPN
eurjchem-1369	9	10	phosphor‐d	phosphor‐d	NOUN
eurjchem-1369	9	11	ibitors	ibitor	NOUN
eurjchem-1369	10	1	[	[	X
eurjchem-1369	10	2	15	15	NUM
eurjchem-1369	10	3	]	]	PUNCT
eurjchem-1369	10	4	.	.	PUNCT
eurjchem-1369	11	1	ylenecyanamid	ylenecyanamid	PROPN
eurjchem-1369	11	2	ctrophilic	ctrophilic	PROPN
eurjchem-1369	11	3	reag	reag	PROPN
eurjchem-1369	11	4	inomethylene	inomethylene	PROPN
eurjchem-1369	11	5	g	g	PROPN
eurjchem-1369	11	6	nds	nds	PROPN
eurjchem-1369	11	7	but	but	CCONJ
eurjchem-1369	11	8	also	also	ADV
eurjchem-1369	11	9	a	a	DET
eurjchem-1369	11	10	c	c	NOUN
eurjchem-1369	11	11	ompounds	ompound	NOUN
eurjchem-1369	12	1	[	[	X
eurjchem-1369	12	2	18	18	NUM
eurjchem-1369	12	3	,	,	PUNCT
eurjchem-1369	12	4	the	the	DET
eurjchem-1369	12	5	action	action	NOUN
eurjchem-1369	12	6	of	of	ADP
eurjchem-1369	12	7	eido‐1h‐pyrazo	eido‐1h‐pyrazo	ADP
eurjchem-1369	12	8	nthesis	nthesis	NOUN
eurjchem-1369	12	9	of	of	ADP
eurjchem-1369	12	10	new	new	ADJ
eurjchem-1369	12	11	atives	ative	NOUN
eurjchem-1369	12	12	.	.	PUNCT
eurjchem-1369	13	1	uropean	uropean	ADJ
eurjchem-1369	13	2	journal	journal	PROPN
eurjchem-1369	13	3	europ	europ	PROPN
eurjchem-1369	13	4	57	57	NUM
eurjchem-1369	13	5	(	(	PUNCT
eurjchem-1369	13	6	online	online	ADJ
eurjchem-1369	13	7	)	)	PUNCT
eurjchem-1369	13	8			NOUN
eurjchem-1369	13	9	20	20	NUM
eurjchem-1369	13	10	tp://dx.doi.org/	tp://dx.doi.org/	NOUN
eurjchem-1369	13	11	pean	pean	PROPN
eurjchem-1369	13	12	jo	jo	PROPN
eurjchem-1369	13	13	journal	journal	PROPN
eurjchem-1369	13	14	web	web	PROPN
eurjchem-1369	13	15	lic	lic	PROPN
eurjchem-1369	13	16	amidin	amidin	PROPN
eurjchem-1369	13	17	es	es	NOUN
eurjchem-1369	13	18	and	and	CCONJ
eurjchem-1369	13	19	py	py	PROPN
eurjchem-1369	13	20	d	d	PROPN
eurjchem-1369	13	21	ahmed	ahmed	PROPN
eurjchem-1369	13	22	m	m	PROPN
eurjchem-1369	13	23	ley	ley	PROPN
eurjchem-1369	13	24	university	university	PROPN
eurjchem-1369	13	25	,	,	PUNCT
eurjchem-1369	13	26	qena	qena	PROPN
eurjchem-1369	13	27	faculty	faculty	NOUN
eurjchem-1369	13	28	of	of	ADP
eurjchem-1369	13	29	science	science	NOUN
eurjchem-1369	13	30	,	,	PUNCT
eurjchem-1369	13	31	s	s	PART
eurjchem-1369	13	32	address	address	NOUN
eurjchem-1369	13	33	:	:	PUNCT
eurjchem-1369	13	34	ahmadbak	ahmadbak	PROPN
eurjchem-1369	13	35	abstract	abstract	ADJ
eurjchem-1369	13	36	n‐bis(methylt	n‐bis(methylt	PROPN
eurjchem-1369	13	37	malononitrile	malononitrile	PROPN
eurjchem-1369	13	38	derivatives	derivative	NOUN
eurjchem-1369	13	39	(	(	PUNCT
eurjchem-1369	13	40	3	3	NUM
eurjchem-1369	13	41	aminopyrazol	aminopyrazol	ADJ
eurjchem-1369	13	42	carboxylic	carboxylic	NOUN
eurjchem-1369	13	43	aci	aci	PROPN
eurjchem-1369	13	44	pyrazolopyrim	pyrazolopyrim	NOUN
eurjchem-1369	13	45	synthesized	synthesize	VERB
eurjchem-1369	13	46	c	c	PROPN
eurjchem-1369	13	47	1h	1h	NUM
eurjchem-1369	13	48	13c	13c	NOUN
eurjchem-1369	13	49	nmr	nmr	NOUN
eurjchem-1369	13	50	an	an	DET
eurjchem-1369	13	51	cite	cite	VERB
eurjchem-1369	13	52	this	this	PRON
eurjchem-1369	13	53	:	:	PUNCT
eurjchem-1369	13	54	eur	eur	ADJ
eurjchem-1369	13	55	.	.	PUNCT
eurjchem-1369	14	1	ermediates	ermediate	NOUN
eurjchem-1369	14	2	for	for	ADP
eurjchem-1369	14	3	yrazole	yrazole	NOUN
eurjchem-1369	14	4	deriva	deriva	PROPN
eurjchem-1369	14	5	been	be	AUX
eurjchem-1369	14	6	establishe	establishe	PROPN
eurjchem-1369	14	7	nes	nes	PROPN
eurjchem-1369	14	8	.	.	PUNCT
eurjchem-1369	15	1	pyrazolo	pyrazolo	PROPN
eurjchem-1369	15	2	[	[	PUNCT
eurjchem-1369	15	3	and	and	CCONJ
eurjchem-1369	15	4	have	have	VERB
eurjchem-1369	15	5	usefu	usefu	ADJ
eurjchem-1369	15	6	iochemical	iochemical	ADJ
eurjchem-1369	15	7	reac	reac	NOUN
eurjchem-1369	15	8	wide	wide	ADJ
eurjchem-1369	15	9	pharmace	pharmace	NOUN
eurjchem-1369	15	10	mal	mal	ADJ
eurjchem-1369	15	11	[	[	X
eurjchem-1369	15	12	4,5	4,5	NUM
eurjchem-1369	15	13	]	]	PUNCT
eurjchem-1369	15	14	,	,	PUNCT
eurjchem-1369	15	15	antisc	antisc	NOUN
eurjchem-1369	15	16	‐viral	‐viral	PROPN
eurjchem-1369	16	1	[	[	X
eurjchem-1369	16	2	9,10	9,10	NUM
eurjchem-1369	16	3	]	]	PUNCT
eurjchem-1369	16	4	,	,	PUNCT
eurjchem-1369	16	5	as	as	ADP
eurjchem-1369	16	6	hibitors	hibitor	NOUN
eurjchem-1369	16	7	[	[	X
eurjchem-1369	16	8	12	12	NUM
eurjchem-1369	16	9	]	]	PUNCT
eurjchem-1369	16	10	,	,	PUNCT
eurjchem-1369	16	11	c	c	PROPN
eurjchem-1369	16	12	diesterase	diesterase	PROPN
eurjchem-1369	16	13	inhi	inhi	PROPN
eurjchem-1369	16	14	de	de	X
eurjchem-1369	16	15	(	(	PUNCT
eurjchem-1369	16	16	1	1	NUM
eurjchem-1369	16	17	)	)	PUNCT
eurjchem-1369	16	18	,	,	PUNCT
eurjchem-1369	16	19	[	[	X
eurjchem-1369	16	20	16,17	16,17	X
eurjchem-1369	16	21	]	]	PUNCT
eurjchem-1369	16	22	gent	gent	NOUN
eurjchem-1369	16	23	for	for	ADP
eurjchem-1369	16	24	the	the	DET
eurjchem-1369	16	25	group	group	NOUN
eurjchem-1369	16	26	of	of	ADP
eurjchem-1369	16	27	amine	amine	ADJ
eurjchem-1369	16	28	c	c	X
eurjchem-1369	16	29	=	=	SYM
eurjchem-1369	16	30	n‐c	n‐c	NOUN
eurjchem-1369	16	31	=	=	ADJ
eurjchem-1369	16	32	n	n	PRON
eurjchem-1369	16	33	unit	unit	NOUN
eurjchem-1369	16	34	,	,	PUNCT
eurjchem-1369	16	35	19	19	NUM
eurjchem-1369	16	36	]	]	PUNCT
eurjchem-1369	16	37	.	.	PUNCT
eurjchem-1369	17	1	the	the	DET
eurjchem-1369	17	2	aim	aim	NOUN
eurjchem-1369	17	3	o	o	X
eurjchem-1369	17	4	several	several	ADJ
eurjchem-1369	17	5	electro	electro	ADJ
eurjchem-1369	17	6	ole‐4‐carboxylic	ole‐4‐carboxylic	PROPN
eurjchem-1369	17	7	pyrazolopyrim	pyrazolopyrim	NOUN
eurjchem-1369	17	8	l	l	PROPN
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eurjchem-1369	17	10	chemistry	chemistry	NOUN
eurjchem-1369	17	11	7	7	NUM
eurjchem-1369	17	12	pean	pean	ADJ
eurjchem-1369	17	13	journal	journal	NOUN
eurjchem-1369	17	14	of	of	ADP
eurjchem-1369	17	15	c	c	PROPN
eurjchem-1369	17	16	016	016	NUM
eurjchem-1369	17	17	atlanta	atlanta	PROPN
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eurjchem-1369	17	19	10.5155	10.5155	NUM
eurjchem-1369	17	20	/	/	SYM
eurjchem-1369	17	21	eurjche	eurjche	NOUN
eurjchem-1369	17	22	ournal	ournal	ADJ
eurjchem-1369	17	23	bpage	bpage	NOUN
eurjchem-1369	17	24	:	:	PUNCT
eurjchem-1369	17	25	www	www	PROPN
eurjchem-1369	17	26	.	.	PUNCT
eurjchem-1369	17	27	nes	nes	PROPN
eurjchem-1369	17	28	:	:	PUNCT
eurjchem-1369	17	29	synth	synth	NOUN
eurjchem-1369	17	30	yrazolo[1	yrazolo[1	PROPN
eurjchem-1369	17	31	,	,	PUNCT
eurjchem-1369	17	32	ohammed	ohamme	VERB
eurjchem-1369	17	33	a	a	DET
eurjchem-1369	17	34	a	a	PRON
eurjchem-1369	17	35	,	,	PUNCT
eurjchem-1369	17	36	83523	83523	NUM
eurjchem-1369	17	37	egypt	egypt	PROPN
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eurjchem-1369	17	40	univer	univer	VERB
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eurjchem-1369	18	1	thio)methylenec	thio)methylenec	DET
eurjchem-1369	18	2	e	e	NOUN
eurjchem-1369	18	3	in	in	ADP
eurjchem-1369	18	4	the	the	DET
eurjchem-1369	18	5	presence	presence	NOUN
eurjchem-1369	18	6	3a	3a	NUM
eurjchem-1369	18	7	,	,	PUNCT
eurjchem-1369	18	8	b	b	NOUN
eurjchem-1369	18	9	)	)	PUNCT
eurjchem-1369	18	10	,	,	PUNCT
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eurjchem-1369	18	15	i	i	PROPN
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eurjchem-1369	18	18	ester	ester	NOUN
eurjchem-1369	18	19	(	(	PUNCT
eurjchem-1369	18	20	4	4	NUM
eurjchem-1369	18	21	midine	midine	NOUN
eurjchem-1369	18	22	and	and	CCONJ
eurjchem-1369	18	23	pyra	pyra	NOUN
eurjchem-1369	18	24	compounds	compound	NOUN
eurjchem-1369	18	25	(	(	PUNCT
eurjchem-1369	18	26	3a	3a	NUM
eurjchem-1369	18	27	,	,	PUNCT
eurjchem-1369	18	28	b	b	PROPN
eurjchem-1369	18	29	nd	nd	NUM
eurjchem-1369	18	30	mass	mass	PROPN
eurjchem-1369	18	31	spectra	spectra	NOUN
eurjchem-1369	18	32	.	.	PUNCT
eurjchem-1369	19	1	j.	j.	PROPN
eurjchem-1369	19	2	chem	chem	PROPN
eurjchem-1369	19	3	.	.	PUNCT
eurjchem-1369	20	1	2016	2016	NUM
eurjchem-1369	20	2	,	,	PUNCT
eurjchem-1369	20	3	r	r	VERB
eurjchem-1369	20	4	the	the	DET
eurjchem-1369	20	5	atives	ative	NOUN
eurjchem-1369	20	6	.	.	PUNCT
eurjchem-1369	21	1	ed	ed	NOUN
eurjchem-1369	21	2	for	for	ADP
eurjchem-1369	21	3	[	[	X
eurjchem-1369	21	4	1,5‐a	1,5‐a	X
eurjchem-1369	21	5	]	]	X
eurjchem-1369	21	6	ul	ul	INTJ
eurjchem-1369	21	7	pro‐	pro‐	PROPN
eurjchem-1369	21	8	ctions	ction	NOUN
eurjchem-1369	21	9	.	.	PUNCT
eurjchem-1369	22	1	eutical	eutical	ADJ
eurjchem-1369	22	2	chisto‐	chisto‐	PROPN
eurjchem-1369	22	3	crf1	crf1	PROPN
eurjchem-1369	22	4	cox‐2	cox‐2	PROPN
eurjchem-1369	22	5	bitors	bitors	PROPN
eurjchem-1369	22	6	is	be	AUX
eurjchem-1369	22	7	an	an	DET
eurjchem-1369	22	8	intro‐	intro‐	NOUN
eurjchem-1369	22	9	es	es	NOUN
eurjchem-1369	22	10	and	and	CCONJ
eurjchem-1369	22	11	in	in	ADP
eurjchem-1369	22	12	the	the	PRON
eurjchem-1369	22	13	of	of	ADP
eurjchem-1369	22	14	this	this	DET
eurjchem-1369	22	15	ophilic	ophilic	NOUN
eurjchem-1369	22	16	c	c	PROPN
eurjchem-1369	22	17	acid	acid	PROPN
eurjchem-1369	22	18	midine	midine	NOUN
eurjchem-1369	22	19	2	2	NUM
eurjchem-1369	22	20	.	.	PUNCT
eurjchem-1369	22	21	e	e	ADP
eurjchem-1369	22	22	2.1	2.1	NUM
eurjchem-1369	22	23	.	.	PUNCT
eurjchem-1369	23	1	elec	elec	PROPN
eurjchem-1369	23	2	reco	reco	PROPN
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eurjchem-1369	23	4	cali	cali	PROPN
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eurjchem-1369	23	6	2.52	2.52	NUM
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eurjchem-1369	23	8	a	a	DET
eurjchem-1369	23	9	s	s	X
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eurjchem-1369	23	12	2.2	2.2	NUM
eurjchem-1369	23	13	.	.	PUNCT
eurjchem-1369	23	14	2.2	2.2	NUM
eurjchem-1369	23	15	.	.	PUNCT
eurjchem-1369	24	1	thio	thio	NOUN
eurjchem-1369	24	2	and	and	CCONJ
eurjchem-1369	24	3	(	(	PUNCT
eurjchem-1369	24	4	1.4	1.4	NUM
eurjchem-1369	24	5	(	(	PUNCT
eurjchem-1369	24	6	0.0	0.0	NUM
eurjchem-1369	24	7	(	(	PUNCT
eurjchem-1369	24	8	1	1	NUM
eurjchem-1369	24	9	)	)	PUNCT
eurjchem-1369	24	10	(	(	PUNCT
eurjchem-1369	24	11	2016	2016	NUM
eurjchem-1369	24	12	)	)	PUNCT
eurjchem-1369	25	1	107‐	107‐	NUM
eurjchem-1369	25	2	chemistry	chemistry	NOUN
eurjchem-1369	25	3	lishing	lishe	VERB
eurjchem-1369	25	4	house	house	NOUN
eurjchem-1369	25	5	ll	ll	PROPN
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eurjchem-1369	25	7	.	.	PUNCT
eurjchem-1369	25	8	of	of	ADP
eurjchem-1369	25	9	che	che	PROPN
eurjchem-1369	25	10	.eurjchem.co	.eurjchem.co	PROPN
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eurjchem-1369	25	13	se	se	PROPN
eurjchem-1369	25	14	5‐a][1,3,5	5‐a][1,3,5	PROPN
eurjchem-1369	25	15	abo‐bakr	abo‐bakr	PROPN
eurjchem-1369	25	16	*	*	PUNCT
eurjchem-1369	25	17	rsity	rsity	NOUN
eurjchem-1369	25	18	,	,	PUNCT
eurjchem-1369	25	19	qena	qena	NOUN
eurjchem-1369	25	20	,	,	PUNCT
eurjchem-1369	25	21	83523	83523	NUM
eurjchem-1369	25	22	e	e	NOUN
eurjchem-1369	25	23	(	(	PUNCT
eurjchem-1369	25	24	a.m.	a.m.	PROPN
eurjchem-1369	25	25	abo‐bakr	abo‐bakr	PROPN
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eurjchem-1369	25	27	.	.	PUNCT
eurjchem-1369	26	1	cyanamide	cyanamide	NOUN
eurjchem-1369	26	2	(	(	PUNCT
eurjchem-1369	26	3	1	1	NUM
eurjchem-1369	26	4	)	)	PUNCT
eurjchem-1369	26	5	w	w	NOUN
eurjchem-1369	26	6	e	e	NOUN
eurjchem-1369	26	7	of	of	ADP
eurjchem-1369	26	8	potassium	potassium	NOUN
eurjchem-1369	26	9	treatment	treatment	NOUN
eurjchem-1369	26	10	with	with	ADP
eurjchem-1369	26	11	(	(	PUNCT
eurjchem-1369	26	12	4a	4a	NUM
eurjchem-1369	26	13	,	,	PUNCT
eurjchem-1369	26	14	b	b	NOUN
eurjchem-1369	26	15	)	)	PUNCT
eurjchem-1369	26	16	.	.	PUNCT
eurjchem-1369	27	1	the	the	DET
eurjchem-1369	27	2	cy	cy	PROPN
eurjchem-1369	27	3	4a	4a	NOUN
eurjchem-1369	27	4	)	)	PUNCT
eurjchem-1369	27	5	is	be	AUX
eurjchem-1369	27	6	found	find	VERB
eurjchem-1369	27	7	to	to	PART
eurjchem-1369	27	8	azolotriazine	azolotriazine	VERB
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eurjchem-1369	27	10	b‐22a	b‐22a	NOUN
eurjchem-1369	27	11	,	,	PUNCT
eurjchem-1369	27	12	b	b	NOUN
eurjchem-1369	27	13	)	)	PUNCT
eurjchem-1369	27	14	were	be	AUX
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eurjchem-1369	27	16	.	.	PUNCT
eurjchem-1369	28	1	7(1	7(1	NUM
eurjchem-1369	28	2	)	)	PUNCT
eurjchem-1369	28	3	,	,	PUNCT
eurjchem-1369	28	4	107‐114	107‐114	PROPN
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eurjchem-1369	28	6	.	.	PUNCT
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eurjchem-1369	29	3	point	point	NOUN
eurjchem-1369	29	4	ctrothermal	ctrothermal	NOUN
eurjchem-1369	29	5	me	i	PRON
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eurjchem-1369	29	7	on	on	ADP
eurjchem-1369	29	8	a	a	DET
eurjchem-1369	29	9	be	be	AUX
eurjchem-1369	29	10	re	re	VERB
eurjchem-1369	29	11	recorded	record	VERB
eurjchem-1369	29	12	ibration	ibration	NOUN
eurjchem-1369	29	13	of	of	ADP
eurjchem-1369	29	14	spec	spec	PROPN
eurjchem-1369	29	15	aks	aks	X
eurjchem-1369	29	16	(	(	PUNCT
eurjchem-1369	29	17	cdcl3	cdcl3	PROPN
eurjchem-1369	29	18	:	:	PUNCT
eurjchem-1369	29	19	δ	δ	PROPN
eurjchem-1369	29	20	1h	1h	NUM
eurjchem-1369	29	21	2	2	NUM
eurjchem-1369	29	22	ppm	ppm	NOUN
eurjchem-1369	29	23	,	,	PUNCT
eurjchem-1369	29	24	13c	13c	NUM
eurjchem-1369	29	25	40	40	NUM
eurjchem-1369	29	26	.	.	PUNCT
eurjchem-1369	30	1	ative	ative	ADJ
eurjchem-1369	30	2	to	to	ADP
eurjchem-1369	30	3	tms	tms	PROPN
eurjchem-1369	30	4	(	(	PUNCT
eurjchem-1369	30	5	1h	1h	NUM
eurjchem-1369	30	6	spectrometer	spectrometer	NOUN
eurjchem-1369	30	7	(	(	PUNCT
eurjchem-1369	30	8	alysis	alysis	NOUN
eurjchem-1369	30	9	was	be	AUX
eurjchem-1369	30	10	car	car	NOUN
eurjchem-1369	30	11	iversity	iversity	NOUN
eurjchem-1369	30	12	.	.	PUNCT
eurjchem-1369	30	13	.	.	PUNCT
eurjchem-1369	31	1	synthesis	synthesis	NOUN
eurjchem-1369	31	2	.1	.1	PROPN
eurjchem-1369	31	3	.	.	PUNCT
eurjchem-1369	32	1	general	general	ADJ
eurjchem-1369	32	2	pro	pro	X
eurjchem-1369	32	3	o)methylenecy	o)methylenecy	PROPN
eurjchem-1369	32	4	d	d	NOUN
eurjchem-1369	32	5	malononitrile	malononitrile	VERB
eurjchem-1369	32	6	a	a	DET
eurjchem-1369	32	7	mixture	mixture	NOUN
eurjchem-1369	32	8	of	of	ADP
eurjchem-1369	32	9	n	n	PROPN
eurjchem-1369	32	10	46	46	NUM
eurjchem-1369	32	11	g	g	NOUN
eurjchem-1369	32	12	,	,	PUNCT
eurjchem-1369	32	13	0.01	0.01	NUM
eurjchem-1369	32	14	mol	mol	ADP
eurjchem-1369	32	15	015	015	NUM
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eurjchem-1369	32	17	)	)	PUNCT
eurjchem-1369	32	18	in	in	ADP
eurjchem-1369	32	19	(	(	PUNCT
eurjchem-1369	32	20	2	2	NUM
eurjchem-1369	32	21	‐114	‐114	NOUN
eurjchem-1369	32	22	lc	lc	NOUN
eurjchem-1369	32	23	‐	‐	NOUN
eurjchem-1369	32	24	all	all	DET
eurjchem-1369	32	25	rights	right	NOUN
eurjchem-1369	32	26	re	re	ADP
eurjchem-1369	32	27	.1369	.1369	PROPN
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eurjchem-1369	32	29	m	m	VERB
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eurjchem-1369	32	31	new	new	ADJ
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eurjchem-1369	33	8	hydr	hydr	NOUN
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eurjchem-1369	33	14	interm	interm	NOUN
eurjchem-1369	33	15	rivatives	rivative	NOUN
eurjchem-1369	33	16	(	(	PUNCT
eurjchem-1369	33	17	5‐22a	5‐22a	NUM
eurjchem-1369	33	18	,	,	PUNCT
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eurjchem-1369	33	23	ts	ts	X
eurjchem-1369	33	24	(	(	PUNCT
eurjchem-1369	33	25	uncorrecte	uncorrecte	NOUN
eurjchem-1369	33	26	elting	elte	VERB
eurjchem-1369	33	27	apparatu	apparatu	PROPN
eurjchem-1369	33	28	ckman	ckman	NOUN
eurjchem-1369	33	29	acculab	acculab	NOUN
eurjchem-1369	33	30	with	with	ADP
eurjchem-1369	33	31	bruker	bruker	PROPN
eurjchem-1369	33	32	ctra	ctra	PROPN
eurjchem-1369	33	33	were	be	AUX
eurjchem-1369	33	34	carri	carri	PROPN
eurjchem-1369	33	35	h	h	NOUN
eurjchem-1369	33	36	7.25	7.25	NUM
eurjchem-1369	33	37	ppm	ppm	NOUN
eurjchem-1369	33	38	,	,	PUNCT
eurjchem-1369	33	39	δ	δ	PROPN
eurjchem-1369	33	40	1	1	NUM
eurjchem-1369	33	41	45	45	NUM
eurjchem-1369	33	42	ppm	ppm	NOUN
eurjchem-1369	33	43	)	)	PUNCT
eurjchem-1369	33	44	.	.	PUNCT
eurjchem-1369	34	1	chem	chem	NOUN
eurjchem-1369	34	2	h	h	NOUN
eurjchem-1369	34	3	,	,	PUNCT
eurjchem-1369	34	4	0.00	0.00	NUM
eurjchem-1369	34	5	ppm	ppm	NOUN
eurjchem-1369	34	6	)	)	PUNCT
eurjchem-1369	34	7	.	.	PUNCT
eurjchem-1369	35	1	m	m	VERB
eurjchem-1369	35	2	(	(	PUNCT
eurjchem-1369	35	3	electron	electron	NOUN
eurjchem-1369	35	4	impa	impa	PROPN
eurjchem-1369	35	5	rried	rrie	VERB
eurjchem-1369	35	6	out	out	ADP
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eurjchem-1369	35	8	m	m	PROPN
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eurjchem-1369	35	12	yananamide	yananamide	NOUN
eurjchem-1369	35	13	(	(	PUNCT
eurjchem-1369	35	14	1	1	NUM
eurjchem-1369	35	15	)	)	PUNCT
eurjchem-1369	35	16	e	e	NOUN
eurjchem-1369	35	17	n‐bis(methylthi	n‐bis(methylthi	ADJ
eurjchem-1369	35	18	e	e	NOUN
eurjchem-1369	35	19	)	)	PUNCT
eurjchem-1369	35	20	and	and	CCONJ
eurjchem-1369	35	21	ethyl	ethyl	PROPN
eurjchem-1369	35	22	cy	cy	PROPN
eurjchem-1369	35	23	0	0	NUM
eurjchem-1369	35	24	ml	ml	NOUN
eurjchem-1369	35	25	)	)	PUNCT
eurjchem-1369	35	26	of	of	ADP
eurjchem-1369	35	27	dimeth	dimeth	PROPN
eurjchem-1369	35	28	served	serve	VERB
eurjchem-1369	35	29	‐	‐	NOUN
eurjchem-1369	35	30	printed	print	VERB
eurjchem-1369	35	31	y	y	PROPN
eurjchem-1369	35	32	w	w	NOUN
eurjchem-1369	35	33	es	es	PROPN
eurjchem-1369	35	34	react	react	VERB
eurjchem-1369	35	35	with	with	ADP
eurjchem-1369	35	36	ethy	ethy	ADJ
eurjchem-1369	35	37	methylsulfoxide	methylsulfoxide	ADJ
eurjchem-1369	35	38	rater	rater	NOUN
eurjchem-1369	35	39	resulted	result	VERB
eurjchem-1369	35	40	th	th	X
eurjchem-1369	35	41	5‐amino‐3‐ureid	5‐amino‐3‐ureid	NUM
eurjchem-1369	35	42	mediate	mediate	NOUN
eurjchem-1369	35	43	for	for	ADP
eurjchem-1369	35	44	the	the	DET
eurjchem-1369	35	45	b	b	NOUN
eurjchem-1369	35	46	)	)	PUNCT
eurjchem-1369	35	47	.	.	PUNCT
eurjchem-1369	36	1	the	the	DET
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eurjchem-1369	36	7	)	)	PUNCT
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eurjchem-1369	36	10	us	we	PRON
eurjchem-1369	36	11	.	.	PUNCT
eurjchem-1369	37	1	the	the	DET
eurjchem-1369	37	2	ir	ir	PROPN
eurjchem-1369	37	3	spect	spect	PROPN
eurjchem-1369	37	4	b	b	PROPN
eurjchem-1369	37	5	1	1	NUM
eurjchem-1369	37	6	.	.	PUNCT
eurjchem-1369	37	7	1h	1h	NUM
eurjchem-1369	37	8	and	and	CCONJ
eurjchem-1369	37	9	13c	13c	NOUN
eurjchem-1369	37	10	ac‐250	ac‐250	PROPN
eurjchem-1369	37	11	spec	spec	PROPN
eurjchem-1369	37	12	ied	ie	VERB
eurjchem-1369	37	13	out	out	ADP
eurjchem-1369	37	14	by	by	ADP
eurjchem-1369	37	15	mea	mea	NOUN
eurjchem-1369	37	16	3c	3c	NUM
eurjchem-1369	37	17	77.00	77.00	NUM
eurjchem-1369	37	18	ppm	ppm	NOUN
eurjchem-1369	37	19	;	;	PUNCT
eurjchem-1369	37	20	mical	mical	ADJ
eurjchem-1369	37	21	shifts	shift	NOUN
eurjchem-1369	37	22	are	be	AUX
eurjchem-1369	37	23	mass	mass	ADJ
eurjchem-1369	37	24	spectra	spectra	NOUN
eurjchem-1369	37	25	we	we	PRON
eurjchem-1369	37	26	act	act	VERB
eurjchem-1369	37	27	)	)	PUNCT
eurjchem-1369	38	1	varian	varian	PROPN
eurjchem-1369	38	2	ch	ch	PROPN
eurjchem-1369	38	3	microanalysis	microanalysis	PROPN
eurjchem-1369	38	4	e	e	NOUN
eurjchem-1369	38	5	reaction	reaction	NOUN
eurjchem-1369	38	6	of	of	ADP
eurjchem-1369	38	7	n‐	n‐	NOUN
eurjchem-1369	38	8	)	)	PUNCT
eurjchem-1369	38	9	with	with	ADP
eurjchem-1369	38	10	ethyl	ethyl	PROPN
eurjchem-1369	38	11	cy	cy	PROPN
eurjchem-1369	38	12	o)methylenecy	o)methylenecy	PROPN
eurjchem-1369	38	13	yanoacetate	yanoacetate	NOUN
eurjchem-1369	38	14	or	or	CCONJ
eurjchem-1369	38	15	hylsulfoxide	hylsulfoxide	VERB
eurjchem-1369	38	16	in	in	ADP
eurjchem-1369	38	17	d	d	PROPN
eurjchem-1369	38	18	in	in	ADP
eurjchem-1369	38	19	the	the	DET
eurjchem-1369	38	20	usa	usa	PROPN
eurjchem-1369	38	21	ylcyanoacetate	ylcyanoacetate	PROPN
eurjchem-1369	38	22	o	o	PROPN
eurjchem-1369	38	23	to	to	PART
eurjchem-1369	38	24	yield	yield	VERB
eurjchem-1369	38	25	the	the	DET
eurjchem-1369	38	26	ure	ure	NOUN
eurjchem-1369	38	27	he	he	PRON
eurjchem-1369	38	28	correspondin	correspondin	VERB
eurjchem-1369	38	29	do‐1h‐pyrazole‐	do‐1h‐pyrazole‐	NOUN
eurjchem-1369	38	30	synthesis	synthesis	NOUN
eurjchem-1369	38	31	of	of	ADP
eurjchem-1369	38	32	ne	ne	PROPN
eurjchem-1369	38	33	l	l	NOUN
eurjchem-1369	38	34	structures	structure	NOUN
eurjchem-1369	38	35	of	of	ADP
eurjchem-1369	38	36	th	th	NUM
eurjchem-1369	38	37	al	al	PROPN
eurjchem-1369	38	38	analyses	analysis	NOUN
eurjchem-1369	38	39	,	,	PUNCT
eurjchem-1369	38	40	ft‐i	ft‐i	PRON
eurjchem-1369	38	41	corded	cord	VERB
eurjchem-1369	38	42	on	on	ADP
eurjchem-1369	38	43	an	an	DET
eurjchem-1369	38	44	tra	tra	NOUN
eurjchem-1369	38	45	(	(	PUNCT
eurjchem-1369	38	46	kbr	kbr	PROPN
eurjchem-1369	38	47	)	)	PUNCT
eurjchem-1369	38	48	were	be	AUX
eurjchem-1369	38	49	c	c	PROPN
eurjchem-1369	38	50	nmr	nmr	NOUN
eurjchem-1369	38	51	spectra	spectra	PROPN
eurjchem-1369	38	52	ctrometer	ctrometer	PROPN
eurjchem-1369	38	53	,	,	PUNCT
eurjchem-1369	38	54	the	the	DET
eurjchem-1369	38	55	ans	an	NOUN
eurjchem-1369	38	56	of	of	ADP
eurjchem-1369	38	57	solvents	solvent	NOUN
eurjchem-1369	38	58	(	(	PUNCT
eurjchem-1369	38	59	cd3)2so	cd3)2so	NOUN
eurjchem-1369	38	60	:	:	PUNCT
eurjchem-1369	38	61	δ	δ	PROPN
eurjchem-1369	38	62	1h	1h	NUM
eurjchem-1369	38	63	e	e	NOUN
eurjchem-1369	38	64	given	give	VERB
eurjchem-1369	38	65	in	in	ADP
eurjchem-1369	38	66	ppm	ppm	PROPN
eurjchem-1369	38	67	ere	ere	PROPN
eurjchem-1369	38	68	recorded	record	VERB
eurjchem-1369	38	69	on	on	ADP
eurjchem-1369	38	70	h‐5	h‐5	PROPN
eurjchem-1369	38	71	.	.	PUNCT
eurjchem-1369	39	1	elemental	elemental	ADJ
eurjchem-1369	39	2	unit	unit	NOUN
eurjchem-1369	39	3	at	at	ADP
eurjchem-1369	39	4	cairo	cairo	PROPN
eurjchem-1369	39	5	‐bis	‐bis	NUM
eurjchem-1369	39	6	(	(	PUNCT
eurjchem-1369	39	7	methyl	methyl	NOUN
eurjchem-1369	39	8	yanoacetate	yanoacetate	PROPN
eurjchem-1369	39	9	yananamide	yananamide	PROPN
eurjchem-1369	39	10	(	(	PUNCT
eurjchem-1369	39	11	1	1	X
eurjchem-1369	39	12	)	)	PUNCT
eurjchem-1369	39	13	r	r	NOUN
eurjchem-1369	39	14	malononitrile	malononitrile	NOUN
eurjchem-1369	39	15	presence	presence	NOUN
eurjchem-1369	39	16	of	of	ADP
eurjchem-1369	39	17	or	or	CCONJ
eurjchem-1369	39	18	ea	ea	NUM
eurjchem-1369	39	19	ng	ng	PROPN
eurjchem-1369	40	1	4‐	4‐	INTJ
eurjchem-1369	41	1	ew	ew	INTJ
eurjchem-1369	41	2	he	he	PRON
eurjchem-1369	41	3	r	r	PROPN
eurjchem-1369	41	4	,	,	PUNCT
eurjchem-1369	41	5	n	n	PROPN
eurjchem-1369	41	6	e	e	X
eurjchem-1369	41	7	a	a	DET
eurjchem-1369	41	8	e	e	X
eurjchem-1369	41	9	s	s	VERB
eurjchem-1369	41	10	h	h	NOUN
eurjchem-1369	41	11	m	m	NOUN
eurjchem-1369	41	12	n	n	ADP
eurjchem-1369	41	13	l	l	NOUN
eurjchem-1369	41	14	o	o	NOUN
eurjchem-1369	41	15	)	)	PUNCT
eurjchem-1369	42	1	e	e	X
eurjchem-1369	42	2	108	108	NUM
eurjchem-1369	42	3	abbas‐temirek	abbas‐temirek	NOUN
eurjchem-1369	42	4	and	and	CCONJ
eurjchem-1369	42	5	abo‐bakr	abo‐bakr	ADJ
eurjchem-1369	42	6	/	/	SYM
eurjchem-1369	42	7	european	european	ADJ
eurjchem-1369	42	8	journal	journal	PROPN
eurjchem-1369	42	9	of	of	ADP
eurjchem-1369	42	10	chemistry	chemistry	NOUN
eurjchem-1369	42	11	7	7	NUM
eurjchem-1369	42	12	(	(	PUNCT
eurjchem-1369	42	13	1	1	NUM
eurjchem-1369	42	14	)	)	PUNCT
eurjchem-1369	42	15	(	(	PUNCT
eurjchem-1369	42	16	2016	2016	NUM
eurjchem-1369	42	17	)	)	PUNCT
eurjchem-1369	43	1	107‐114	107‐114	NUM
eurjchem-1369	43	2	scheme	scheme	NOUN
eurjchem-1369	43	3	1	1	NUM
eurjchem-1369	43	4	potassium	potassium	NOUN
eurjchem-1369	43	5	carbonate	carbonate	NOUN
eurjchem-1369	43	6	(	(	PUNCT
eurjchem-1369	43	7	2.7	2.7	NUM
eurjchem-1369	43	8	g	g	NOUN
eurjchem-1369	43	9	,	,	PUNCT
eurjchem-1369	43	10	0.02	0.02	NUM
eurjchem-1369	43	11	mole	mole	NOUN
eurjchem-1369	43	12	)	)	PUNCT
eurjchem-1369	43	13	was	be	AUX
eurjchem-1369	43	14	stirred	stir	VERB
eurjchem-1369	43	15	at	at	ADP
eurjchem-1369	43	16	room	room	NOUN
eurjchem-1369	43	17	temperature	temperature	NOUN
eurjchem-1369	43	18	for	for	ADP
eurjchem-1369	43	19	4	4	NUM
eurjchem-1369	43	20	h.	h.	NOUN
eurjchem-1369	43	21	the	the	DET
eurjchem-1369	43	22	reaction	reaction	NOUN
eurjchem-1369	43	23	mixture	mixture	NOUN
eurjchem-1369	43	24	was	be	AUX
eurjchem-1369	43	25	poured	pour	VERB
eurjchem-1369	43	26	portion	portion	NOUN
eurjchem-1369	43	27	wise	wise	ADJ
eurjchem-1369	43	28	into	into	ADP
eurjchem-1369	43	29	50	50	NUM
eurjchem-1369	43	30	ml	ml	NOUN
eurjchem-1369	43	31	of	of	ADP
eurjchem-1369	43	32	10	10	NUM
eurjchem-1369	43	33	%	%	NOUN
eurjchem-1369	43	34	hydrochloric	hydrochloric	ADJ
eurjchem-1369	43	35	acid	acid	NOUN
eurjchem-1369	43	36	containing	contain	VERB
eurjchem-1369	43	37	crushed	crush	VERB
eurjchem-1369	43	38	ice	ice	NOUN
eurjchem-1369	43	39	.	.	PUNCT
eurjchem-1369	44	1	the	the	DET
eurjchem-1369	44	2	obtained	obtain	VERB
eurjchem-1369	44	3	precipitate	precipitate	NOUN
eurjchem-1369	44	4	was	be	AUX
eurjchem-1369	44	5	collected	collect	VERB
eurjchem-1369	44	6	by	by	ADP
eurjchem-1369	44	7	filtration	filtration	NOUN
eurjchem-1369	44	8	and	and	CCONJ
eurjchem-1369	44	9	crystallized	crystallize	VERB
eurjchem-1369	44	10	from	from	ADP
eurjchem-1369	44	11	appropriate	appropriate	ADJ
eurjchem-1369	44	12	solvent	solvent	NOUN
eurjchem-1369	44	13	to	to	PART
eurjchem-1369	44	14	yield	yield	VERB
eurjchem-1369	44	15	compound	compound	NOUN
eurjchem-1369	44	16	3a	3a	PROPN
eurjchem-1369	44	17	and	and	CCONJ
eurjchem-1369	44	18	3b	3b	NUM
eurjchem-1369	44	19	,	,	PUNCT
eurjchem-1369	44	20	respectively	respectively	ADV
eurjchem-1369	44	21	(	(	PUNCT
eurjchem-1369	44	22	scheme	scheme	NOUN
eurjchem-1369	44	23	1	1	NUM
eurjchem-1369	44	24	)	)	PUNCT
eurjchem-1369	44	25	.	.	PUNCT
eurjchem-1369	45	1	2‐cyano‐3‐methylsulfanyl‐3‐ureido‐acrylic	2‐cyano‐3‐methylsulfanyl‐3‐ureido‐acrylic	PROPN
eurjchem-1369	45	2	acid	acid	PROPN
eurjchem-1369	45	3	ethyl	ethyl	PROPN
eurjchem-1369	45	4	ester	ester	NOUN
eurjchem-1369	45	5	(	(	PUNCT
eurjchem-1369	45	6	3a	3a	NUM
eurjchem-1369	45	7	):	):	PUNCT
eurjchem-1369	45	8	color	color	NOUN
eurjchem-1369	45	9	:	:	PUNCT
eurjchem-1369	45	10	colourless	colourless	ADJ
eurjchem-1369	45	11	needles	needle	NOUN
eurjchem-1369	45	12	.	.	PUNCT
eurjchem-1369	46	1	yield	yield	NOUN
eurjchem-1369	46	2	:	:	PUNCT
eurjchem-1369	46	3	85	85	NUM
eurjchem-1369	46	4	%	%	NOUN
eurjchem-1369	46	5	.	.	PUNCT
eurjchem-1369	47	1	m.p	m.p	PROPN
eurjchem-1369	47	2	.	.	PROPN
eurjchem-1369	47	3	:	:	PUNCT
eurjchem-1369	48	1	225‐227	225‐227	NUM
eurjchem-1369	48	2	°	°	ADP
eurjchem-1369	48	3	c	c	X
eurjchem-1369	48	4	.	.	PUNCT
eurjchem-1369	48	5	ft‐ir	ft‐ir	NOUN
eurjchem-1369	48	6	(	(	PUNCT
eurjchem-1369	48	7	kbr	kbr	PROPN
eurjchem-1369	48	8	,	,	PUNCT
eurjchem-1369	48	9			PROPN
eurjchem-1369	48	10	,	,	PUNCT
eurjchem-1369	48	11	cm‐1	cm‐1	PROPN
eurjchem-1369	48	12	):	):	PUNCT
eurjchem-1369	48	13	3414	3414	NUM
eurjchem-1369	48	14	(	(	PUNCT
eurjchem-1369	48	15	nh2	nh2	PROPN
eurjchem-1369	48	16	)	)	PUNCT
eurjchem-1369	48	17	,	,	PUNCT
eurjchem-1369	48	18	3283	3283	NUM
eurjchem-1369	48	19	(	(	PUNCT
eurjchem-1369	48	20	nh	nh	NOUN
eurjchem-1369	48	21	)	)	PUNCT
eurjchem-1369	48	22	,	,	PUNCT
eurjchem-1369	48	23	2214	2214	NUM
eurjchem-1369	48	24	(	(	PUNCT
eurjchem-1369	48	25	cn	cn	PROPN
eurjchem-1369	48	26	)	)	PUNCT
eurjchem-1369	48	27	,	,	PUNCT
eurjchem-1369	48	28	1700	1700	NUM
eurjchem-1369	48	29	,	,	PUNCT
eurjchem-1369	48	30	1689	1689	NUM
eurjchem-1369	48	31	(	(	PUNCT
eurjchem-1369	48	32	c	c	X
eurjchem-1369	48	33	=	=	SYM
eurjchem-1369	48	34	o	o	NOUN
eurjchem-1369	48	35	's	's	PART
eurjchem-1369	48	36	)	)	PUNCT
eurjchem-1369	48	37	.	.	PUNCT
eurjchem-1369	49	1	1h	1h	NUM
eurjchem-1369	49	2	nmr	nmr	NOUN
eurjchem-1369	49	3	(	(	PUNCT
eurjchem-1369	49	4	250	250	NUM
eurjchem-1369	49	5	mhz	mhz	NOUN
eurjchem-1369	49	6	,	,	PUNCT
eurjchem-1369	49	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	49	8	,	,	PUNCT
eurjchem-1369	49	9	δ	δ	PROPN
eurjchem-1369	49	10	,	,	PUNCT
eurjchem-1369	49	11	ppm	ppm	NUM
eurjchem-1369	49	12	):	):	PUNCT
eurjchem-1369	49	13	1.23‐1.37	1.23‐1.37	PROPN
eurjchem-1369	49	14	(	(	PUNCT
eurjchem-1369	49	15	t	t	PROPN
eurjchem-1369	49	16	,	,	PUNCT
eurjchem-1369	49	17	3h	3h	NUM
eurjchem-1369	49	18	,	,	PUNCT
eurjchem-1369	49	19	ch3	ch3	PROPN
eurjchem-1369	49	20	)	)	PUNCT
eurjchem-1369	49	21	,	,	PUNCT
eurjchem-1369	49	22	2.54	2.54	NUM
eurjchem-1369	49	23	(	(	PUNCT
eurjchem-1369	49	24	s	s	PROPN
eurjchem-1369	49	25	,	,	PUNCT
eurjchem-1369	49	26	3h	3h	NUM
eurjchem-1369	49	27	,	,	PUNCT
eurjchem-1369	49	28	s‐me	s‐me	NOUN
eurjchem-1369	49	29	)	)	PUNCT
eurjchem-1369	49	30	,	,	PUNCT
eurjchem-1369	49	31	4.10‐4.18	4.10‐4.18	PROPN
eurjchem-1369	49	32	(	(	PUNCT
eurjchem-1369	49	33	q	q	NOUN
eurjchem-1369	49	34	,	,	PUNCT
eurjchem-1369	49	35	2h	2h	NUM
eurjchem-1369	49	36	,	,	PUNCT
eurjchem-1369	49	37	‐ch2	‐ch2	NUM
eurjchem-1369	49	38	)	)	PUNCT
eurjchem-1369	49	39	,	,	PUNCT
eurjchem-1369	49	40	7.07	7.07	NUM
eurjchem-1369	49	41	(	(	PUNCT
eurjchem-1369	49	42	br.s	br.s	PROPN
eurjchem-1369	49	43	,	,	PUNCT
eurjchem-1369	49	44	2h	2h	NUM
eurjchem-1369	49	45	,	,	PUNCT
eurjchem-1369	49	46	nh2	nh2	PROPN
eurjchem-1369	49	47	)	)	PUNCT
eurjchem-1369	49	48	,	,	PUNCT
eurjchem-1369	49	49	10.21	10.21	NUM
eurjchem-1369	49	50	(	(	PUNCT
eurjchem-1369	49	51	s	s	PROPN
eurjchem-1369	49	52	,	,	PUNCT
eurjchem-1369	49	53	1h	1h	NUM
eurjchem-1369	49	54	,	,	PUNCT
eurjchem-1369	49	55	nh	nh	PROPN
eurjchem-1369	49	56	)	)	PUNCT
eurjchem-1369	49	57	.	.	PUNCT
eurjchem-1369	50	1	13c	13c	NOUN
eurjchem-1369	50	2	nmr	nmr	NOUN
eurjchem-1369	50	3	(	(	PUNCT
eurjchem-1369	50	4	75	75	NUM
eurjchem-1369	50	5	mhz	mhz	NOUN
eurjchem-1369	50	6	,	,	PUNCT
eurjchem-1369	50	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	50	8	,	,	PUNCT
eurjchem-1369	50	9	δ	δ	PROPN
eurjchem-1369	50	10	,	,	PUNCT
eurjchem-1369	50	11	ppm	ppm	NUM
eurjchem-1369	50	12	):	):	PUNCT
eurjchem-1369	50	13	14.27	14.27	NUM
eurjchem-1369	50	14	(	(	PUNCT
eurjchem-1369	50	15	1c	1c	NOUN
eurjchem-1369	50	16	,	,	PUNCT
eurjchem-1369	50	17	sch3	sch3	PROPN
eurjchem-1369	50	18	)	)	PUNCT
eurjchem-1369	50	19	,	,	PUNCT
eurjchem-1369	50	20	16.26	16.26	NUM
eurjchem-1369	50	21	(	(	PUNCT
eurjchem-1369	50	22	1c	1c	NOUN
eurjchem-1369	50	23	,	,	PUNCT
eurjchem-1369	50	24	ch3	ch3	PROPN
eurjchem-1369	50	25	)	)	PUNCT
eurjchem-1369	50	26	,	,	PUNCT
eurjchem-1369	50	27	60.98	60.98	NUM
eurjchem-1369	50	28	(	(	PUNCT
eurjchem-1369	50	29	1c	1c	NOUN
eurjchem-1369	50	30	,	,	PUNCT
eurjchem-1369	50	31	ch2	ch2	PROPN
eurjchem-1369	50	32	)	)	PUNCT
eurjchem-1369	50	33	,	,	PUNCT
eurjchem-1369	50	34	67.21	67.21	NUM
eurjchem-1369	50	35	(	(	PUNCT
eurjchem-1369	50	36	1c	1c	NOUN
eurjchem-1369	50	37	,	,	PUNCT
eurjchem-1369	50	38	=	=	NOUN
eurjchem-1369	50	39	c‐cn	c‐cn	NOUN
eurjchem-1369	50	40	)	)	PUNCT
eurjchem-1369	50	41	,	,	PUNCT
eurjchem-1369	50	42	116.76	116.76	NUM
eurjchem-1369	50	43	(	(	PUNCT
eurjchem-1369	50	44	1c	1c	NOUN
eurjchem-1369	50	45	,	,	PUNCT
eurjchem-1369	50	46	cn	cn	PROPN
eurjchem-1369	50	47	)	)	PUNCT
eurjchem-1369	50	48	,	,	PUNCT
eurjchem-1369	50	49	152.20	152.20	NUM
eurjchem-1369	50	50	(	(	PUNCT
eurjchem-1369	50	51	1c	1c	NOUN
eurjchem-1369	50	52	,	,	PUNCT
eurjchem-1369	50	53	conh2	conh2	PROPN
eurjchem-1369	50	54	)	)	PUNCT
eurjchem-1369	50	55	,	,	PUNCT
eurjchem-1369	50	56	163.68	163.68	NUM
eurjchem-1369	50	57	(	(	PUNCT
eurjchem-1369	50	58	1c	1c	NOUN
eurjchem-1369	50	59	,	,	PUNCT
eurjchem-1369	50	60	cooet	cooet	NOUN
eurjchem-1369	50	61	)	)	PUNCT
eurjchem-1369	50	62	,	,	PUNCT
eurjchem-1369	50	63	169.35	169.35	NUM
eurjchem-1369	50	64	(	(	PUNCT
eurjchem-1369	50	65	1c	1c	NOUN
eurjchem-1369	50	66	,	,	PUNCT
eurjchem-1369	50	67	=	=	NOUN
eurjchem-1369	50	68	c‐sme	c‐sme	ADJ
eurjchem-1369	50	69	)	)	PUNCT
eurjchem-1369	50	70	.	.	PUNCT
eurjchem-1369	51	1	ms	ms	NOUN
eurjchem-1369	51	2	(	(	PUNCT
eurjchem-1369	51	3	ei	ei	PROPN
eurjchem-1369	51	4	,	,	PUNCT
eurjchem-1369	51	5	m	m	PROPN
eurjchem-1369	51	6	/	/	SYM
eurjchem-1369	51	7	z	z	PROPN
eurjchem-1369	51	8	(	(	PUNCT
eurjchem-1369	51	9	%	%	NOUN
eurjchem-1369	51	10	)	)	PUNCT
eurjchem-1369	51	11	):	):	PUNCT
eurjchem-1369	51	12	229	229	NUM
eurjchem-1369	51	13	(	(	PUNCT
eurjchem-1369	51	14	m+	m+	NUM
eurjchem-1369	51	15	,	,	PUNCT
eurjchem-1369	51	16	31	31	NUM
eurjchem-1369	51	17	)	)	PUNCT
eurjchem-1369	51	18	.	.	PUNCT
eurjchem-1369	52	1	anal	anal	PROPN
eurjchem-1369	52	2	.	.	PUNCT
eurjchem-1369	52	3	calcd	calcd	NOUN
eurjchem-1369	52	4	.	.	PUNCT
eurjchem-1369	53	1	for	for	ADP
eurjchem-1369	53	2	c8h11n3o3s	c8h11n3o3s	ADJ
eurjchem-1369	53	3	:	:	PUNCT
eurjchem-1369	54	1	c	c	X
eurjchem-1369	54	2	,	,	PUNCT
eurjchem-1369	54	3	41.91	41.91	NUM
eurjchem-1369	54	4	;	;	PUNCT
eurjchem-1369	54	5	h	h	X
eurjchem-1369	54	6	,	,	PUNCT
eurjchem-1369	54	7	4.84	4.84	NUM
eurjchem-1369	54	8	;	;	PUNCT
eurjchem-1369	54	9	n	n	CCONJ
eurjchem-1369	54	10	,	,	PUNCT
eurjchem-1369	54	11	18.33	18.33	NUM
eurjchem-1369	54	12	;	;	PUNCT
eurjchem-1369	54	13	s	s	PROPN
eurjchem-1369	54	14	,	,	PUNCT
eurjchem-1369	54	15	13.99	13.99	NUM
eurjchem-1369	54	16	.	.	PUNCT
eurjchem-1369	54	17	found	find	VERB
eurjchem-1369	54	18	:	:	PUNCT
eurjchem-1369	55	1	c	c	X
eurjchem-1369	55	2	,	,	PUNCT
eurjchem-1369	55	3	42.45	42.45	NUM
eurjchem-1369	55	4	;	;	PUNCT
eurjchem-1369	55	5	h	h	NOUN
eurjchem-1369	55	6	,	,	PUNCT
eurjchem-1369	55	7	4.88	4.88	NUM
eurjchem-1369	55	8	;	;	PUNCT
eurjchem-1369	55	9	n	n	CCONJ
eurjchem-1369	55	10	,	,	PUNCT
eurjchem-1369	55	11	17.98	17.98	NUM
eurjchem-1369	55	12	;	;	PUNCT
eurjchem-1369	55	13	s	s	NOUN
eurjchem-1369	55	14	,	,	PUNCT
eurjchem-1369	55	15	13.75	13.75	NUM
eurjchem-1369	55	16	%	%	NOUN
eurjchem-1369	55	17	.	.	PUNCT
eurjchem-1369	56	1	(	(	PUNCT
eurjchem-1369	56	2	2,2‐dicyano‐1‐methylsulfanyl‐vinyl)‐urea	2,2‐dicyano‐1‐methylsulfanyl‐vinyl)‐urea	NUM
eurjchem-1369	56	3	(	(	PUNCT
eurjchem-1369	56	4	3b	3b	NUM
eurjchem-1369	56	5	):	):	PUNCT
eurjchem-1369	56	6	color	color	NOUN
eurjchem-1369	56	7	:	:	PUNCT
eurjchem-1369	56	8	buff	buff	PROPN
eurjchem-1369	56	9	crystals	crystal	NOUN
eurjchem-1369	56	10	.	.	PUNCT
eurjchem-1369	57	1	yield	yield	NOUN
eurjchem-1369	57	2	:	:	PUNCT
eurjchem-1369	57	3	83	83	NUM
eurjchem-1369	57	4	%	%	NOUN
eurjchem-1369	57	5	.	.	PUNCT
eurjchem-1369	58	1	m.p	m.p	PROPN
eurjchem-1369	58	2	.	.	PROPN
eurjchem-1369	58	3	:	:	PUNCT
eurjchem-1369	59	1	295‐297	295‐297	NUM
eurjchem-1369	59	2	°	°	ADP
eurjchem-1369	59	3	c	c	X
eurjchem-1369	59	4	.	.	PUNCT
eurjchem-1369	60	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	60	2	(	(	PUNCT
eurjchem-1369	60	3	kbr	kbr	PROPN
eurjchem-1369	60	4	,	,	PUNCT
eurjchem-1369	60	5			PROPN
eurjchem-1369	60	6	,	,	PUNCT
eurjchem-1369	60	7	cm‐1	cm‐1	PROPN
eurjchem-1369	60	8	):	):	PUNCT
eurjchem-1369	60	9	3341‐3446	3341‐3446	NUM
eurjchem-1369	60	10	(	(	PUNCT
eurjchem-1369	60	11	nh2	nh2	PROPN
eurjchem-1369	60	12	)	)	PUNCT
eurjchem-1369	60	13	,	,	PUNCT
eurjchem-1369	60	14	3223	3223	NUM
eurjchem-1369	60	15	(	(	PUNCT
eurjchem-1369	60	16	nh	nh	PROPN
eurjchem-1369	60	17	)	)	PUNCT
eurjchem-1369	60	18	,	,	PUNCT
eurjchem-1369	60	19	2203‐2214	2203‐2214	NUM
eurjchem-1369	60	20	(	(	PUNCT
eurjchem-1369	60	21	2cn	2cn	ADJ
eurjchem-1369	60	22	)	)	PUNCT
eurjchem-1369	60	23	,	,	PUNCT
eurjchem-1369	60	24	1673	1673	NUM
eurjchem-1369	60	25	(	(	PUNCT
eurjchem-1369	60	26	c	c	NOUN
eurjchem-1369	60	27	=	=	PRON
eurjchem-1369	60	28	o)(amide	o)(amide	NUM
eurjchem-1369	60	29	)	)	PUNCT
eurjchem-1369	60	30	.	.	PUNCT
eurjchem-1369	61	1	1h	1h	NUM
eurjchem-1369	61	2	nmr	nmr	NOUN
eurjchem-1369	61	3	(	(	PUNCT
eurjchem-1369	61	4	250	250	NUM
eurjchem-1369	61	5	mhz	mhz	NOUN
eurjchem-1369	61	6	,	,	PUNCT
eurjchem-1369	61	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	61	8	,	,	PUNCT
eurjchem-1369	61	9	δ	δ	PROPN
eurjchem-1369	61	10	,	,	PUNCT
eurjchem-1369	61	11	ppm	ppm	NUM
eurjchem-1369	61	12	):	):	PUNCT
eurjchem-1369	61	13	2.5	2.5	NUM
eurjchem-1369	61	14	(	(	PUNCT
eurjchem-1369	61	15	s	s	PROPN
eurjchem-1369	61	16	,	,	PUNCT
eurjchem-1369	61	17	3h	3h	NUM
eurjchem-1369	61	18	,	,	PUNCT
eurjchem-1369	61	19	sme	sme	NOUN
eurjchem-1369	61	20	)	)	PUNCT
eurjchem-1369	61	21	,	,	PUNCT
eurjchem-1369	61	22	7.6‐7.93	7.6‐7.93	NUM
eurjchem-1369	61	23	(	(	PUNCT
eurjchem-1369	61	24	br.s	br.s	PROPN
eurjchem-1369	61	25	,	,	PUNCT
eurjchem-1369	61	26	2h	2h	NUM
eurjchem-1369	61	27	,	,	PUNCT
eurjchem-1369	61	28	nh2	nh2	PROPN
eurjchem-1369	61	29	)	)	PUNCT
eurjchem-1369	61	30	,	,	PUNCT
eurjchem-1369	61	31	10.95	10.95	NUM
eurjchem-1369	61	32	(	(	PUNCT
eurjchem-1369	61	33	s	s	PROPN
eurjchem-1369	61	34	,	,	PUNCT
eurjchem-1369	61	35	1h	1h	NUM
eurjchem-1369	61	36	,	,	PUNCT
eurjchem-1369	61	37	nh	nh	PROPN
eurjchem-1369	61	38	)	)	PUNCT
eurjchem-1369	61	39	.	.	PUNCT
eurjchem-1369	62	1	13c	13c	NOUN
eurjchem-1369	62	2	nmr	nmr	NOUN
eurjchem-1369	62	3	(	(	PUNCT
eurjchem-1369	62	4	75	75	NUM
eurjchem-1369	62	5	mhz	mhz	NOUN
eurjchem-1369	62	6	,	,	PUNCT
eurjchem-1369	62	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	62	8	,	,	PUNCT
eurjchem-1369	62	9	δ	δ	PROPN
eurjchem-1369	62	10	,	,	PUNCT
eurjchem-1369	62	11	ppm	ppm	NUM
eurjchem-1369	62	12	):	):	PUNCT
eurjchem-1369	62	13	12.61	12.61	NUM
eurjchem-1369	62	14	(	(	PUNCT
eurjchem-1369	62	15	1c	1c	NOUN
eurjchem-1369	62	16	,	,	PUNCT
eurjchem-1369	62	17	sch3	sch3	PROPN
eurjchem-1369	62	18	)	)	PUNCT
eurjchem-1369	62	19	,	,	PUNCT
eurjchem-1369	62	20	115.12	115.12	NUM
eurjchem-1369	62	21	(	(	PUNCT
eurjchem-1369	62	22	1c	1c	NOUN
eurjchem-1369	62	23	,	,	PUNCT
eurjchem-1369	62	24	=	=	NOUN
eurjchem-1369	62	25	c‐	c‐	NOUN
eurjchem-1369	62	26	cn	cn	PROPN
eurjchem-1369	62	27	)	)	PUNCT
eurjchem-1369	62	28	,	,	PUNCT
eurjchem-1369	62	29	143.42	143.42	NUM
eurjchem-1369	62	30	(	(	PUNCT
eurjchem-1369	62	31	1c	1c	X
eurjchem-1369	62	32	,	,	PUNCT
eurjchem-1369	62	33	cn	cn	PROPN
eurjchem-1369	62	34	)	)	PUNCT
eurjchem-1369	62	35	,	,	PUNCT
eurjchem-1369	62	36	153.07	153.07	NUM
eurjchem-1369	62	37	(	(	PUNCT
eurjchem-1369	62	38	1c	1c	X
eurjchem-1369	62	39	,	,	PUNCT
eurjchem-1369	62	40	cn	cn	PROPN
eurjchem-1369	62	41	)	)	PUNCT
eurjchem-1369	62	42	,	,	PUNCT
eurjchem-1369	62	43	158.55	158.55	NUM
eurjchem-1369	62	44	(	(	PUNCT
eurjchem-1369	62	45	1c	1c	NOUN
eurjchem-1369	62	46	,	,	PUNCT
eurjchem-1369	62	47	conh2	conh2	PROPN
eurjchem-1369	62	48	)	)	PUNCT
eurjchem-1369	62	49	,	,	PUNCT
eurjchem-1369	62	50	176.49	176.49	NUM
eurjchem-1369	62	51	(	(	PUNCT
eurjchem-1369	62	52	1c	1c	NOUN
eurjchem-1369	62	53	,	,	PUNCT
eurjchem-1369	62	54	=	=	NOUN
eurjchem-1369	62	55	c‐sme	c‐sme	ADJ
eurjchem-1369	62	56	)	)	PUNCT
eurjchem-1369	62	57	.	.	PUNCT
eurjchem-1369	63	1	ms	ms	NOUN
eurjchem-1369	63	2	(	(	PUNCT
eurjchem-1369	63	3	ei	ei	PROPN
eurjchem-1369	63	4	,	,	PUNCT
eurjchem-1369	63	5	m	m	PROPN
eurjchem-1369	63	6	/	/	SYM
eurjchem-1369	63	7	z	z	PROPN
eurjchem-1369	63	8	(	(	PUNCT
eurjchem-1369	63	9	%	%	NOUN
eurjchem-1369	63	10	)	)	PUNCT
eurjchem-1369	63	11	):	):	PUNCT
eurjchem-1369	63	12	182	182	NUM
eurjchem-1369	63	13	(	(	PUNCT
eurjchem-1369	63	14	m+	m+	NUM
eurjchem-1369	63	15	,	,	PUNCT
eurjchem-1369	63	16	43	43	NUM
eurjchem-1369	63	17	)	)	PUNCT
eurjchem-1369	63	18	.	.	PUNCT
eurjchem-1369	64	1	anal	anal	PROPN
eurjchem-1369	64	2	.	.	PUNCT
eurjchem-1369	64	3	calcd	calcd	NOUN
eurjchem-1369	64	4	.	.	PUNCT
eurjchem-1369	65	1	for	for	ADP
eurjchem-1369	65	2	c6h6n4os	c6h6n4o	NOUN
eurjchem-1369	65	3	:	:	PUNCT
eurjchem-1369	65	4	c	c	X
eurjchem-1369	65	5	,	,	PUNCT
eurjchem-1369	65	6	39.55	39.55	NUM
eurjchem-1369	65	7	;	;	PUNCT
eurjchem-1369	65	8	h	h	NOUN
eurjchem-1369	65	9	,	,	PUNCT
eurjchem-1369	65	10	3.32	3.32	NUM
eurjchem-1369	65	11	;	;	PUNCT
eurjchem-1369	65	12	n	n	CCONJ
eurjchem-1369	65	13	,	,	PUNCT
eurjchem-1369	65	14	30.75	30.75	NUM
eurjchem-1369	65	15	;	;	PUNCT
eurjchem-1369	65	16	s	s	X
eurjchem-1369	65	17	,	,	PUNCT
eurjchem-1369	65	18	17.60	17.60	NUM
eurjchem-1369	65	19	.	.	PUNCT
eurjchem-1369	65	20	found	find	VERB
eurjchem-1369	65	21	:	:	PUNCT
eurjchem-1369	66	1	c	c	X
eurjchem-1369	66	2	,	,	PUNCT
eurjchem-1369	66	3	39.73	39.73	NUM
eurjchem-1369	66	4	;	;	PUNCT
eurjchem-1369	66	5	h	h	NOUN
eurjchem-1369	66	6	,	,	PUNCT
eurjchem-1369	66	7	3.61	3.61	NUM
eurjchem-1369	66	8	;	;	PUNCT
eurjchem-1369	66	9	n	n	CCONJ
eurjchem-1369	66	10	,	,	PUNCT
eurjchem-1369	66	11	30.43	30.43	NUM
eurjchem-1369	66	12	;	;	PUNCT
eurjchem-1369	66	13	s	s	X
eurjchem-1369	66	14	,	,	PUNCT
eurjchem-1369	66	15	17.34	17.34	NUM
eurjchem-1369	66	16	%	%	NOUN
eurjchem-1369	66	17	.	.	PUNCT
eurjchem-1369	67	1	2.2.2	2.2.2	X
eurjchem-1369	67	2	.	.	PUNCT
eurjchem-1369	67	3	general	general	ADJ
eurjchem-1369	67	4	procedure	procedure	NOUN
eurjchem-1369	67	5	for	for	ADP
eurjchem-1369	67	6	the	the	DET
eurjchem-1369	67	7	reaction	reaction	NOUN
eurjchem-1369	67	8	of	of	ADP
eurjchem-1369	67	9	3a	3a	NUM
eurjchem-1369	67	10	and	and	CCONJ
eurjchem-1369	67	11	3b	3b	NUM
eurjchem-1369	67	12	with	with	ADP
eurjchem-1369	67	13	hydrazine	hydrazine	NOUN
eurjchem-1369	67	14	hydrate	hydrate	VERB
eurjchem-1369	67	15	a	a	DET
eurjchem-1369	67	16	mixture	mixture	NOUN
eurjchem-1369	67	17	of	of	ADP
eurjchem-1369	67	18	compound	compound	NOUN
eurjchem-1369	67	19	3a	3a	PROPN
eurjchem-1369	67	20	or	or	CCONJ
eurjchem-1369	67	21	3b	3b	NUM
eurjchem-1369	67	22	(	(	PUNCT
eurjchem-1369	67	23	0.01	0.01	NUM
eurjchem-1369	67	24	mole	mole	NOUN
eurjchem-1369	67	25	)	)	PUNCT
eurjchem-1369	67	26	,	,	PUNCT
eurjchem-1369	67	27	hydrazine	hydrazine	NOUN
eurjchem-1369	67	28	hydrate	hydrate	NOUN
eurjchem-1369	67	29	(	(	PUNCT
eurjchem-1369	67	30	1	1	NUM
eurjchem-1369	67	31	ml	ml	NOUN
eurjchem-1369	67	32	)	)	PUNCT
eurjchem-1369	67	33	in	in	ADP
eurjchem-1369	67	34	20	20	NUM
eurjchem-1369	67	35	ml	ml	NOUN
eurjchem-1369	67	36	ethanol	ethanol	NOUN
eurjchem-1369	67	37	was	be	AUX
eurjchem-1369	67	38	stirred	stir	VERB
eurjchem-1369	67	39	at	at	ADP
eurjchem-1369	67	40	room	room	NOUN
eurjchem-1369	67	41	temperature	temperature	NOUN
eurjchem-1369	67	42	for	for	ADP
eurjchem-1369	67	43	4	4	NUM
eurjchem-1369	67	44	h.	h.	NOUN
eurjchem-1369	67	45	the	the	DET
eurjchem-1369	67	46	solvent	solvent	NOUN
eurjchem-1369	67	47	was	be	AUX
eurjchem-1369	67	48	removed	remove	VERB
eurjchem-1369	67	49	under	under	ADP
eurjchem-1369	67	50	reduced	reduce	VERB
eurjchem-1369	67	51	pressure	pressure	NOUN
eurjchem-1369	67	52	and	and	CCONJ
eurjchem-1369	67	53	the	the	DET
eurjchem-1369	67	54	solid	solid	ADJ
eurjchem-1369	67	55	formed	form	VERB
eurjchem-1369	67	56	was	be	AUX
eurjchem-1369	67	57	crystallized	crystallize	VERB
eurjchem-1369	67	58	from	from	ADP
eurjchem-1369	67	59	appropriate	appropriate	ADJ
eurjchem-1369	67	60	solvent	solvent	NOUN
eurjchem-1369	67	61	to	to	PART
eurjchem-1369	67	62	yield	yield	VERB
eurjchem-1369	67	63	compound	compound	NOUN
eurjchem-1369	67	64	4a	4a	NOUN
eurjchem-1369	67	65	and	and	CCONJ
eurjchem-1369	67	66	4b	4b	PROPN
eurjchem-1369	67	67	,	,	PUNCT
eurjchem-1369	67	68	respect‐	respect‐	VERB
eurjchem-1369	67	69	tively	tively	ADV
eurjchem-1369	67	70	(	(	PUNCT
eurjchem-1369	67	71	scheme	scheme	NOUN
eurjchem-1369	67	72	1	1	NUM
eurjchem-1369	67	73	)	)	PUNCT
eurjchem-1369	67	74	.	.	PUNCT
eurjchem-1369	68	1	5‐amino‐3‐ureido‐1h‐pyrazole‐4‐carboxylic	5‐amino‐3‐ureido‐1h‐pyrazole‐4‐carboxylic	NUM
eurjchem-1369	68	2	acid	acid	PROPN
eurjchem-1369	68	3	ethyl	ethyl	PROPN
eurjchem-1369	68	4	ester	ester	NOUN
eurjchem-1369	68	5	(	(	PUNCT
eurjchem-1369	68	6	4a	4a	NUM
eurjchem-1369	68	7	):	):	PUNCT
eurjchem-1369	68	8	color	color	NOUN
eurjchem-1369	68	9	:	:	PUNCT
eurjchem-1369	68	10	colourless	colourless	ADJ
eurjchem-1369	68	11	needles	needle	NOUN
eurjchem-1369	68	12	.	.	PUNCT
eurjchem-1369	69	1	yield	yield	NOUN
eurjchem-1369	69	2	:	:	PUNCT
eurjchem-1369	69	3	61	61	NUM
eurjchem-1369	69	4	%	%	NOUN
eurjchem-1369	69	5	.	.	PUNCT
eurjchem-1369	70	1	m.p	m.p	PROPN
eurjchem-1369	70	2	.	.	PROPN
eurjchem-1369	70	3	:	:	PUNCT
eurjchem-1369	71	1	246‐248	246‐248	NUM
eurjchem-1369	71	2	°	°	ADP
eurjchem-1369	71	3	c	c	X
eurjchem-1369	71	4	.	.	PUNCT
eurjchem-1369	72	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	72	2	(	(	PUNCT
eurjchem-1369	72	3	kbr	kbr	PROPN
eurjchem-1369	72	4	,	,	PUNCT
eurjchem-1369	72	5			PROPN
eurjchem-1369	72	6	,	,	PUNCT
eurjchem-1369	72	7	cm‐1	cm‐1	PROPN
eurjchem-1369	72	8	):	):	PUNCT
eurjchem-1369	72	9	3358‐3491	3358‐3491	NUM
eurjchem-1369	72	10	(	(	PUNCT
eurjchem-1369	72	11	2nh2	2nh2	NUM
eurjchem-1369	72	12	)	)	PUNCT
eurjchem-1369	72	13	,	,	PUNCT
eurjchem-1369	72	14	3212	3212	NUM
eurjchem-1369	72	15	(	(	PUNCT
eurjchem-1369	72	16	nh	nh	PROPN
eurjchem-1369	72	17	)	)	PUNCT
eurjchem-1369	72	18	,	,	PUNCT
eurjchem-1369	72	19	1691‐	1691‐	NUM
eurjchem-1369	72	20	1647	1647	NUM
eurjchem-1369	72	21	(	(	PUNCT
eurjchem-1369	72	22	c	c	X
eurjchem-1369	72	23	=	=	SYM
eurjchem-1369	72	24	o	o	NOUN
eurjchem-1369	72	25	's	's	PART
eurjchem-1369	72	26	)	)	PUNCT
eurjchem-1369	72	27	.	.	PUNCT
eurjchem-1369	73	1	1h	1h	NUM
eurjchem-1369	73	2	nmr	nmr	NOUN
eurjchem-1369	73	3	(	(	PUNCT
eurjchem-1369	73	4	250	250	NUM
eurjchem-1369	73	5	mhz	mhz	NOUN
eurjchem-1369	73	6	,	,	PUNCT
eurjchem-1369	73	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	73	8	,	,	PUNCT
eurjchem-1369	73	9	δ	δ	PROPN
eurjchem-1369	73	10	,	,	PUNCT
eurjchem-1369	73	11	ppm	ppm	NUM
eurjchem-1369	73	12	):	):	PUNCT
eurjchem-1369	73	13	1.21‐1.27	1.21‐1.27	NUM
eurjchem-1369	73	14	(	(	PUNCT
eurjchem-1369	73	15	t	t	PROPN
eurjchem-1369	73	16	,	,	PUNCT
eurjchem-1369	73	17	3h	3h	NUM
eurjchem-1369	73	18	,	,	PUNCT
eurjchem-1369	73	19	ch3	ch3	PROPN
eurjchem-1369	73	20	)	)	PUNCT
eurjchem-1369	73	21	,	,	PUNCT
eurjchem-1369	73	22	4.15‐4.23	4.15‐4.23	X
eurjchem-1369	73	23	(	(	PUNCT
eurjchem-1369	73	24	q	q	NOUN
eurjchem-1369	73	25	,	,	PUNCT
eurjchem-1369	73	26	2h	2h	NUM
eurjchem-1369	73	27	,	,	PUNCT
eurjchem-1369	73	28	‐ch2	‐ch2	NUM
eurjchem-1369	73	29	)	)	PUNCT
eurjchem-1369	73	30	,	,	PUNCT
eurjchem-1369	73	31	6.12	6.12	NUM
eurjchem-1369	73	32	(	(	PUNCT
eurjchem-1369	73	33	br.s	br.s	PROPN
eurjchem-1369	73	34	,	,	PUNCT
eurjchem-1369	73	35	2h	2h	NUM
eurjchem-1369	73	36	,	,	PUNCT
eurjchem-1369	73	37	‐nh2	‐nh2	NUM
eurjchem-1369	73	38	)	)	PUNCT
eurjchem-1369	73	39	,	,	PUNCT
eurjchem-1369	73	40	7.1	7.1	NUM
eurjchem-1369	73	41	(	(	PUNCT
eurjchem-1369	73	42	br.s	br.s	PROPN
eurjchem-1369	73	43	,	,	PUNCT
eurjchem-1369	73	44	2h	2h	NUM
eurjchem-1369	73	45	,	,	PUNCT
eurjchem-1369	73	46	nh2	nh2	PROPN
eurjchem-1369	73	47	)	)	PUNCT
eurjchem-1369	73	48	,	,	PUNCT
eurjchem-1369	73	49	7.67	7.67	NUM
eurjchem-1369	73	50	(	(	PUNCT
eurjchem-1369	73	51	s	s	PROPN
eurjchem-1369	73	52	,	,	PUNCT
eurjchem-1369	73	53	1h	1h	NUM
eurjchem-1369	73	54	,	,	PUNCT
eurjchem-1369	73	55	nh	nh	PROPN
eurjchem-1369	73	56	)	)	PUNCT
eurjchem-1369	73	57	,	,	PUNCT
eurjchem-1369	73	58	11.34	11.34	NUM
eurjchem-1369	73	59	(	(	PUNCT
eurjchem-1369	73	60	s	s	PROPN
eurjchem-1369	73	61	,	,	PUNCT
eurjchem-1369	73	62	1h	1h	NUM
eurjchem-1369	73	63	,	,	PUNCT
eurjchem-1369	73	64	nh	nh	PROPN
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eurjchem-1369	73	66	.	.	PUNCT
eurjchem-1369	74	1	13c	13c	NOUN
eurjchem-1369	74	2	nmr	nmr	NOUN
eurjchem-1369	74	3	(	(	PUNCT
eurjchem-1369	74	4	75	75	NUM
eurjchem-1369	74	5	mhz	mhz	NOUN
eurjchem-1369	74	6	,	,	PUNCT
eurjchem-1369	74	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	74	8	,	,	PUNCT
eurjchem-1369	74	9	δ	δ	PROPN
eurjchem-1369	74	10	,	,	PUNCT
eurjchem-1369	74	11	ppm	ppm	NUM
eurjchem-1369	74	12	):	):	PUNCT
eurjchem-1369	74	13	14.29	14.29	NUM
eurjchem-1369	74	14	(	(	PUNCT
eurjchem-1369	74	15	1c	1c	NOUN
eurjchem-1369	74	16	,	,	PUNCT
eurjchem-1369	74	17	ch3	ch3	PROPN
eurjchem-1369	74	18	)	)	PUNCT
eurjchem-1369	74	19	,	,	PUNCT
eurjchem-1369	74	20	14.60	14.60	NUM
eurjchem-1369	74	21	(	(	PUNCT
eurjchem-1369	74	22	1c	1c	NOUN
eurjchem-1369	74	23	,	,	PUNCT
eurjchem-1369	74	24	=	=	NOUN
eurjchem-1369	74	25	c‐nh2	c‐nh2	PROPN
eurjchem-1369	74	26	)	)	PUNCT
eurjchem-1369	74	27	,	,	PUNCT
eurjchem-1369	74	28	38.69	38.69	NUM
eurjchem-1369	74	29	(	(	PUNCT
eurjchem-1369	74	30	1c	1c	X
eurjchem-1369	74	31	,	,	PUNCT
eurjchem-1369	74	32	n	n	CCONJ
eurjchem-1369	74	33	=	=	NOUN
eurjchem-1369	74	34	c‐nh	c‐nh	NOUN
eurjchem-1369	74	35	)	)	PUNCT
eurjchem-1369	74	36	,	,	PUNCT
eurjchem-1369	74	37	59.25	59.25	NUM
eurjchem-1369	74	38	(	(	PUNCT
eurjchem-1369	74	39	1c	1c	NOUN
eurjchem-1369	74	40	,	,	PUNCT
eurjchem-1369	74	41	ch2	ch2	PROPN
eurjchem-1369	74	42	)	)	PUNCT
eurjchem-1369	74	43	,	,	PUNCT
eurjchem-1369	74	44	60.95	60.95	NUM
eurjchem-1369	74	45	(	(	PUNCT
eurjchem-1369	74	46	1c	1c	NOUN
eurjchem-1369	74	47	,	,	PUNCT
eurjchem-1369	74	48	=	=	PRON
eurjchem-1369	74	49	c‐cooet	c‐cooet	NOUN
eurjchem-1369	74	50	,	,	PUNCT
eurjchem-1369	74	51	154.59	154.59	NUM
eurjchem-1369	74	52	(	(	PUNCT
eurjchem-1369	74	53	1c	1c	NOUN
eurjchem-1369	74	54	,	,	PUNCT
eurjchem-1369	74	55	conh2	conh2	PROPN
eurjchem-1369	74	56	)	)	PUNCT
eurjchem-1369	74	57	,	,	PUNCT
eurjchem-1369	74	58	163.98	163.98	NUM
eurjchem-1369	74	59	(	(	PUNCT
eurjchem-1369	74	60	1c	1c	NOUN
eurjchem-1369	74	61	,	,	PUNCT
eurjchem-1369	74	62	cooet	cooet	NOUN
eurjchem-1369	74	63	)	)	PUNCT
eurjchem-1369	74	64	.	.	PUNCT
eurjchem-1369	75	1	ms	ms	NOUN
eurjchem-1369	75	2	(	(	PUNCT
eurjchem-1369	75	3	ei	ei	PROPN
eurjchem-1369	75	4	,	,	PUNCT
eurjchem-1369	75	5	m	m	PROPN
eurjchem-1369	75	6	/	/	SYM
eurjchem-1369	75	7	z	z	PROPN
eurjchem-1369	75	8	(	(	PUNCT
eurjchem-1369	75	9	%	%	NOUN
eurjchem-1369	75	10	)	)	PUNCT
eurjchem-1369	75	11	):	):	PUNCT
eurjchem-1369	75	12	213	213	NUM
eurjchem-1369	75	13	(	(	PUNCT
eurjchem-1369	75	14	m+	m+	NUM
eurjchem-1369	75	15	,	,	PUNCT
eurjchem-1369	75	16	66	66	NUM
eurjchem-1369	75	17	)	)	PUNCT
eurjchem-1369	75	18	.	.	PUNCT
eurjchem-1369	76	1	anal	anal	PROPN
eurjchem-1369	76	2	.	.	PUNCT
eurjchem-1369	76	3	calcd	calcd	NOUN
eurjchem-1369	76	4	.	.	PUNCT
eurjchem-1369	77	1	for	for	ADP
eurjchem-1369	77	2	c7h11n5o3	c7h11n5o3	NOUN
eurjchem-1369	77	3	:	:	PUNCT
eurjchem-1369	77	4	c	c	X
eurjchem-1369	77	5	,	,	PUNCT
eurjchem-1369	77	6	39.44	39.44	NUM
eurjchem-1369	77	7	;	;	PUNCT
eurjchem-1369	77	8	h	h	X
eurjchem-1369	77	9	,	,	PUNCT
eurjchem-1369	77	10	5.20	5.20	NUM
eurjchem-1369	77	11	;	;	PUNCT
eurjchem-1369	77	12	n	n	CCONJ
eurjchem-1369	77	13	,	,	PUNCT
eurjchem-1369	77	14	32.85	32.85	NUM
eurjchem-1369	77	15	.	.	PUNCT
eurjchem-1369	77	16	found	find	VERB
eurjchem-1369	77	17	;	;	PUNCT
eurjchem-1369	77	18	c	c	X
eurjchem-1369	77	19	,	,	PUNCT
eurjchem-1369	77	20	39.41	39.41	NUM
eurjchem-1369	77	21	;	;	PUNCT
eurjchem-1369	78	1	h	h	NOUN
eurjchem-1369	78	2	,	,	PUNCT
eurjchem-1369	78	3	4.95	4.95	NUM
eurjchem-1369	78	4	;	;	PUNCT
eurjchem-1369	78	5	n	n	CCONJ
eurjchem-1369	78	6	,	,	PUNCT
eurjchem-1369	78	7	32.78	32.78	NUM
eurjchem-1369	78	8	%	%	NOUN
eurjchem-1369	78	9	.	.	PUNCT
eurjchem-1369	79	1	(	(	PUNCT
eurjchem-1369	79	2	5‐amino‐4‐cyano‐1h‐pyrazol‐3‐yl)‐urea	5‐amino‐4‐cyano‐1h‐pyrazol‐3‐yl)‐urea	NUM
eurjchem-1369	79	3	(	(	PUNCT
eurjchem-1369	79	4	4b	4b	X
eurjchem-1369	79	5	):	):	PUNCT
eurjchem-1369	79	6	color	color	PROPN
eurjchem-1369	79	7	:	:	PUNCT
eurjchem-1369	79	8	buff	buff	PROPN
eurjchem-1369	79	9	crystals	crystal	NOUN
eurjchem-1369	79	10	.	.	PUNCT
eurjchem-1369	80	1	yield	yield	NOUN
eurjchem-1369	80	2	:	:	PUNCT
eurjchem-1369	80	3	48	48	NUM
eurjchem-1369	80	4	%	%	NOUN
eurjchem-1369	80	5	.	.	PUNCT
eurjchem-1369	81	1	m.p	m.p	PROPN
eurjchem-1369	81	2	.	.	PROPN
eurjchem-1369	81	3	:	:	PUNCT
eurjchem-1369	82	1	262‐264	262‐264	NOUN
eurjchem-1369	82	2	°	°	PROPN
eurjchem-1369	82	3	c	c	X
eurjchem-1369	82	4	.	.	PUNCT
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eurjchem-1369	83	2	(	(	PUNCT
eurjchem-1369	83	3	kbr	kbr	PROPN
eurjchem-1369	83	4	,	,	PUNCT
eurjchem-1369	83	5			PROPN
eurjchem-1369	83	6	,	,	PUNCT
eurjchem-1369	83	7	cm‐1	cm‐1	PROPN
eurjchem-1369	83	8	):	):	PUNCT
eurjchem-1369	83	9	3357‐3479	3357‐3479	NUM
eurjchem-1369	83	10	(	(	PUNCT
eurjchem-1369	83	11	2nh2	2nh2	NUM
eurjchem-1369	83	12	)	)	PUNCT
eurjchem-1369	83	13	,	,	PUNCT
eurjchem-1369	83	14	3280	3280	NUM
eurjchem-1369	83	15	(	(	PUNCT
eurjchem-1369	83	16	nh	nh	NOUN
eurjchem-1369	83	17	)	)	PUNCT
eurjchem-1369	83	18	,	,	PUNCT
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eurjchem-1369	83	20	(	(	PUNCT
eurjchem-1369	83	21	cn	cn	PROPN
eurjchem-1369	83	22	)	)	PUNCT
eurjchem-1369	83	23	,	,	PUNCT
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eurjchem-1369	83	25	(	(	PUNCT
eurjchem-1369	83	26	c	c	NOUN
eurjchem-1369	83	27	=	=	NOUN
eurjchem-1369	83	28	o	o	NOUN
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eurjchem-1369	83	30	(	(	PUNCT
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eurjchem-1369	83	32	)	)	PUNCT
eurjchem-1369	83	33	.	.	PUNCT
eurjchem-1369	84	1	1h	1h	NUM
eurjchem-1369	84	2	nmr	nmr	NOUN
eurjchem-1369	84	3	(	(	PUNCT
eurjchem-1369	84	4	250	250	NUM
eurjchem-1369	84	5	mhz	mhz	NOUN
eurjchem-1369	84	6	,	,	PUNCT
eurjchem-1369	84	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	84	8	,	,	PUNCT
eurjchem-1369	84	9	δ	δ	PROPN
eurjchem-1369	84	10	,	,	PUNCT
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eurjchem-1369	84	12	):	):	PUNCT
eurjchem-1369	84	13	6.18	6.18	NUM
eurjchem-1369	84	14	(	(	PUNCT
eurjchem-1369	84	15	br.s	br.s	PROPN
eurjchem-1369	84	16	,	,	PUNCT
eurjchem-1369	84	17	2h	2h	NUM
eurjchem-1369	84	18	,	,	PUNCT
eurjchem-1369	84	19	nh2	nh2	PROPN
eurjchem-1369	84	20	)	)	PUNCT
eurjchem-1369	84	21	,	,	PUNCT
eurjchem-1369	84	22	6.4	6.4	NUM
eurjchem-1369	84	23	(	(	PUNCT
eurjchem-1369	84	24	br.s	br.s	PROPN
eurjchem-1369	84	25	,	,	PUNCT
eurjchem-1369	84	26	2h	2h	NUM
eurjchem-1369	84	27	,	,	PUNCT
eurjchem-1369	84	28	nh2	nh2	PROPN
eurjchem-1369	84	29	)	)	PUNCT
eurjchem-1369	84	30	,	,	PUNCT
eurjchem-1369	84	31	11.5	11.5	NUM
eurjchem-1369	84	32	(	(	PUNCT
eurjchem-1369	84	33	s	s	PROPN
eurjchem-1369	84	34	,	,	PUNCT
eurjchem-1369	84	35	1h	1h	NUM
eurjchem-1369	84	36	,	,	PUNCT
eurjchem-1369	84	37	nh	nh	PROPN
eurjchem-1369	84	38	)	)	PUNCT
eurjchem-1369	84	39	,	,	PUNCT
eurjchem-1369	84	40	12.15	12.15	NUM
eurjchem-1369	84	41	(	(	PUNCT
eurjchem-1369	84	42	s	s	PROPN
eurjchem-1369	84	43	,	,	PUNCT
eurjchem-1369	84	44	1h	1h	NUM
eurjchem-1369	84	45	,	,	PUNCT
eurjchem-1369	84	46	nh	nh	PROPN
eurjchem-1369	84	47	)	)	PUNCT
eurjchem-1369	84	48	.	.	PUNCT
eurjchem-1369	85	1	ms	ms	NOUN
eurjchem-1369	85	2	(	(	PUNCT
eurjchem-1369	85	3	ei	ei	PROPN
eurjchem-1369	85	4	,	,	PUNCT
eurjchem-1369	85	5	m	m	PROPN
eurjchem-1369	85	6	/	/	SYM
eurjchem-1369	85	7	z	z	PROPN
eurjchem-1369	85	8	(	(	PUNCT
eurjchem-1369	85	9	%	%	NOUN
eurjchem-1369	85	10	)	)	PUNCT
eurjchem-1369	85	11	):	):	PUNCT
eurjchem-1369	85	12	166	166	NUM
eurjchem-1369	85	13	(	(	PUNCT
eurjchem-1369	85	14	m+	m+	NUM
eurjchem-1369	85	15	,	,	PUNCT
eurjchem-1369	85	16	33	33	NUM
eurjchem-1369	85	17	)	)	PUNCT
eurjchem-1369	85	18	.	.	PUNCT
eurjchem-1369	86	1	anal	anal	PROPN
eurjchem-1369	86	2	.	.	PUNCT
eurjchem-1369	86	3	calcd	calcd	NOUN
eurjchem-1369	86	4	.	.	PUNCT
eurjchem-1369	87	1	for	for	SCONJ
eurjchem-1369	87	2	c5h6n6o	c5h6n6o	PROPN
eurjchem-1369	87	3	:	:	PUNCT
eurjchem-1369	87	4	c	c	X
eurjchem-1369	87	5	,	,	PUNCT
eurjchem-1369	87	6	36.15	36.15	NUM
eurjchem-1369	87	7	;	;	PUNCT
eurjchem-1369	87	8	h	h	NOUN
eurjchem-1369	87	9	,	,	PUNCT
eurjchem-1369	87	10	3.64	3.64	NUM
eurjchem-1369	87	11	;	;	PUNCT
eurjchem-1369	87	12	n	n	CCONJ
eurjchem-1369	87	13	,	,	PUNCT
eurjchem-1369	87	14	50.58	50.58	NUM
eurjchem-1369	87	15	.	.	PUNCT
eurjchem-1369	87	16	found	find	VERB
eurjchem-1369	87	17	:	:	PUNCT
eurjchem-1369	88	1	c	c	X
eurjchem-1369	88	2	,	,	PUNCT
eurjchem-1369	88	3	36.41	36.41	NUM
eurjchem-1369	88	4	;	;	PUNCT
eurjchem-1369	88	5	h	h	X
eurjchem-1369	88	6	,	,	PUNCT
eurjchem-1369	88	7	3.47	3.47	NUM
eurjchem-1369	88	8	;	;	PUNCT
eurjchem-1369	88	9	n	n	CCONJ
eurjchem-1369	88	10	,	,	PUNCT
eurjchem-1369	88	11	50.43	50.43	NUM
eurjchem-1369	88	12	%	%	NOUN
eurjchem-1369	88	13	.	.	PUNCT
eurjchem-1369	89	1	2.2.3	2.2.3	X
eurjchem-1369	89	2	.	.	PUNCT
eurjchem-1369	89	3	general	general	ADJ
eurjchem-1369	89	4	procedure	procedure	NOUN
eurjchem-1369	89	5	for	for	ADP
eurjchem-1369	89	6	the	the	DET
eurjchem-1369	89	7	synthesis	synthesis	NOUN
eurjchem-1369	89	8	of	of	ADP
eurjchem-1369	89	9	pyrazolo[1,5‐a	pyrazolo[1,5‐a	NOUN
eurjchem-1369	89	10	]	]	PUNCT
eurjchem-1369	89	11	pyrimidines	pyrimidine	NOUN
eurjchem-1369	89	12	5	5	NUM
eurjchem-1369	89	13	and	and	CCONJ
eurjchem-1369	89	14	6a	6a	NOUN
eurjchem-1369	89	15	,	,	PUNCT
eurjchem-1369	89	16	b	b	NOUN
eurjchem-1369	89	17	to	to	ADP
eurjchem-1369	89	18	a	a	DET
eurjchem-1369	89	19	solution	solution	NOUN
eurjchem-1369	89	20	of	of	ADP
eurjchem-1369	89	21	compound	compound	NOUN
eurjchem-1369	89	22	4a	4a	NOUN
eurjchem-1369	89	23	(	(	PUNCT
eurjchem-1369	89	24	2.13	2.13	NUM
eurjchem-1369	89	25	g	g	NOUN
eurjchem-1369	89	26	,	,	PUNCT
eurjchem-1369	89	27	0.01	0.01	NUM
eurjchem-1369	89	28	mole	mole	NOUN
eurjchem-1369	89	29	)	)	PUNCT
eurjchem-1369	89	30	in	in	ADP
eurjchem-1369	89	31	(	(	PUNCT
eurjchem-1369	89	32	10	10	NUM
eurjchem-1369	89	33	ml	ml	NOUN
eurjchem-1369	89	34	)	)	PUNCT
eurjchem-1369	89	35	acetic	acetic	ADJ
eurjchem-1369	89	36	acid	acid	NOUN
eurjchem-1369	89	37	,	,	PUNCT
eurjchem-1369	89	38	(	(	PUNCT
eurjchem-1369	89	39	0.01	0.01	NUM
eurjchem-1369	89	40	mole	mole	NOUN
eurjchem-1369	89	41	)	)	PUNCT
eurjchem-1369	89	42	of	of	ADP
eurjchem-1369	89	43	acetylacetone	acetylacetone	NOUN
eurjchem-1369	89	44	,	,	PUNCT
eurjchem-1369	89	45	ethylaceto	ethylaceto	NOUN
eurjchem-1369	89	46	acetate	acetate	NOUN
eurjchem-1369	89	47	or	or	CCONJ
eurjchem-1369	89	48	diethyl‐3‐oxo‐gluturate	diethyl‐3‐oxo‐gluturate	PROPN
eurjchem-1369	89	49	)	)	PUNCT
eurjchem-1369	89	50	was	be	AUX
eurjchem-1369	89	51	added	add	VERB
eurjchem-1369	89	52	.	.	PUNCT
eurjchem-1369	90	1	the	the	DET
eurjchem-1369	90	2	reaction	reaction	NOUN
eurjchem-1369	90	3	mixture	mixture	NOUN
eurjchem-1369	90	4	was	be	AUX
eurjchem-1369	90	5	refluxed	refluxe	VERB
eurjchem-1369	90	6	for	for	ADP
eurjchem-1369	90	7	the	the	DET
eurjchem-1369	90	8	appropriate	appropriate	ADJ
eurjchem-1369	90	9	time	time	NOUN
eurjchem-1369	90	10	(	(	PUNCT
eurjchem-1369	90	11	7‐14	7‐14	NUM
eurjchem-1369	90	12	h	h	NOUN
eurjchem-1369	90	13	)	)	PUNCT
eurjchem-1369	90	14	.	.	PUNCT
eurjchem-1369	91	1	after	after	ADP
eurjchem-1369	91	2	cooling	cool	VERB
eurjchem-1369	91	3	the	the	DET
eurjchem-1369	91	4	reaction	reaction	NOUN
eurjchem-1369	91	5	mixture	mixture	NOUN
eurjchem-1369	91	6	was	be	AUX
eurjchem-1369	91	7	poured	pour	VERB
eurjchem-1369	91	8	into	into	ADP
eurjchem-1369	91	9	water	water	NOUN
eurjchem-1369	91	10	.	.	PUNCT
eurjchem-1369	92	1	the	the	DET
eurjchem-1369	92	2	solid	solid	ADJ
eurjchem-1369	92	3	product	product	NOUN
eurjchem-1369	92	4	formed	form	VERB
eurjchem-1369	92	5	crystallized	crystallize	VERB
eurjchem-1369	92	6	from	from	ADP
eurjchem-1369	92	7	appropriate	appropriate	ADJ
eurjchem-1369	92	8	solvent	solvent	NOUN
eurjchem-1369	92	9	to	to	PART
eurjchem-1369	92	10	yield	yield	VERB
eurjchem-1369	92	11	compound	compound	NOUN
eurjchem-1369	92	12	5	5	NUM
eurjchem-1369	92	13	,	,	PUNCT
eurjchem-1369	92	14	6a	6a	NOUN
eurjchem-1369	92	15	and	and	CCONJ
eurjchem-1369	92	16	6b	6b	NOUN
eurjchem-1369	92	17	,	,	PUNCT
eurjchem-1369	92	18	respectively	respectively	ADV
eurjchem-1369	92	19	(	(	PUNCT
eurjchem-1369	92	20	scheme	scheme	NOUN
eurjchem-1369	92	21	2	2	NUM
eurjchem-1369	92	22	)	)	PUNCT
eurjchem-1369	92	23	.	.	PUNCT
eurjchem-1369	93	1	5,7‐dimethyl‐2‐ureido‐pyrazolo[1	5,7‐dimethyl‐2‐ureido‐pyrazolo[1	PROPN
eurjchem-1369	93	2	,	,	PUNCT
eurjchem-1369	93	3	5‐a]pyrimidine‐3‐carboxy	5‐a]pyrimidine‐3‐carboxy	PROPN
eurjchem-1369	93	4	lic	lic	PROPN
eurjchem-1369	93	5	acid	acid	PROPN
eurjchem-1369	93	6	ethyl	ethyl	PROPN
eurjchem-1369	93	7	ester	ester	NOUN
eurjchem-1369	93	8	(	(	PUNCT
eurjchem-1369	93	9	5	5	NUM
eurjchem-1369	93	10	):	):	PUNCT
eurjchem-1369	93	11	color	color	NOUN
eurjchem-1369	93	12	:	:	PUNCT
eurjchem-1369	93	13	buff	buff	PROPN
eurjchem-1369	93	14	crystals	crystal	NOUN
eurjchem-1369	93	15	.	.	PUNCT
eurjchem-1369	94	1	yield	yield	NOUN
eurjchem-1369	94	2	:	:	PUNCT
eurjchem-1369	94	3	56	56	NUM
eurjchem-1369	94	4	%	%	NOUN
eurjchem-1369	94	5	.	.	PUNCT
eurjchem-1369	95	1	m.p	m.p	PROPN
eurjchem-1369	95	2	.	.	PROPN
eurjchem-1369	95	3	:	:	PUNCT
eurjchem-1369	96	1	289‐270	289‐270	NUM
eurjchem-1369	96	2	°	°	SYM
eurjchem-1369	96	3	c	c	NOUN
eurjchem-1369	96	4	.	.	PUNCT
eurjchem-1369	97	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	97	2	(	(	PUNCT
eurjchem-1369	97	3	kbr	kbr	PROPN
eurjchem-1369	97	4	,	,	PUNCT
eurjchem-1369	97	5			PROPN
eurjchem-1369	97	6	,	,	PUNCT
eurjchem-1369	97	7	cm‐1	cm‐1	PROPN
eurjchem-1369	97	8	):	):	PUNCT
eurjchem-1369	97	9	3369‐3478	3369‐3478	NUM
eurjchem-1369	97	10	(	(	PUNCT
eurjchem-1369	97	11	nh2	nh2	PROPN
eurjchem-1369	97	12	)	)	PUNCT
eurjchem-1369	97	13	,	,	PUNCT
eurjchem-1369	97	14	3229	3229	NUM
eurjchem-1369	97	15	(	(	PUNCT
eurjchem-1369	97	16	nh	nh	NOUN
eurjchem-1369	97	17	)	)	PUNCT
eurjchem-1369	97	18	,	,	PUNCT
eurjchem-1369	97	19	1693	1693	NUM
eurjchem-1369	97	20	,	,	PUNCT
eurjchem-1369	97	21	1660	1660	NUM
eurjchem-1369	97	22	(	(	PUNCT
eurjchem-1369	97	23	c	c	X
eurjchem-1369	97	24	=	=	SYM
eurjchem-1369	97	25	o	o	NOUN
eurjchem-1369	97	26	's	's	PART
eurjchem-1369	97	27	)	)	PUNCT
eurjchem-1369	97	28	.	.	PUNCT
eurjchem-1369	98	1	1h	1h	NUM
eurjchem-1369	98	2	nmr	nmr	NOUN
eurjchem-1369	98	3	(	(	PUNCT
eurjchem-1369	98	4	250	250	NUM
eurjchem-1369	98	5	mhz	mhz	NOUN
eurjchem-1369	98	6	,	,	PUNCT
eurjchem-1369	98	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	98	8	,	,	PUNCT
eurjchem-1369	98	9	δ	δ	PROPN
eurjchem-1369	98	10	,	,	PUNCT
eurjchem-1369	98	11	ppm	ppm	NUM
eurjchem-1369	98	12	):	):	PUNCT
eurjchem-1369	98	13	1.3	1.3	NUM
eurjchem-1369	98	14	(	(	PUNCT
eurjchem-1369	98	15	t	t	PROPN
eurjchem-1369	98	16	,	,	PUNCT
eurjchem-1369	98	17	3h	3h	NUM
eurjchem-1369	98	18	,	,	PUNCT
eurjchem-1369	98	19	ch3	ch3	PROPN
eurjchem-1369	98	20	)	)	PUNCT
eurjchem-1369	98	21	,	,	PUNCT
eurjchem-1369	98	22	2.13	2.13	NUM
eurjchem-1369	98	23	(	(	PUNCT
eurjchem-1369	98	24	s	s	PROPN
eurjchem-1369	98	25	,	,	PUNCT
eurjchem-1369	98	26	3h	3h	NUM
eurjchem-1369	98	27	,	,	PUNCT
eurjchem-1369	98	28	ch3	ch3	PROPN
eurjchem-1369	98	29	)	)	PUNCT
eurjchem-1369	98	30	,	,	PUNCT
eurjchem-1369	98	31	2.27	2.27	NUM
eurjchem-1369	98	32	(	(	PUNCT
eurjchem-1369	98	33	s	s	PROPN
eurjchem-1369	98	34	,	,	PUNCT
eurjchem-1369	98	35	3h	3h	NUM
eurjchem-1369	98	36	,	,	PUNCT
eurjchem-1369	98	37	ch3	ch3	PROPN
eurjchem-1369	98	38	)	)	PUNCT
eurjchem-1369	98	39	,	,	PUNCT
eurjchem-1369	98	40	4.18	4.18	NUM
eurjchem-1369	98	41	(	(	PUNCT
eurjchem-1369	98	42	q	q	NOUN
eurjchem-1369	98	43	,	,	PUNCT
eurjchem-1369	98	44	2h	2h	NUM
eurjchem-1369	98	45	,	,	PUNCT
eurjchem-1369	98	46	ch2	ch2	PROPN
eurjchem-1369	98	47	)	)	PUNCT
eurjchem-1369	98	48	,	,	PUNCT
eurjchem-1369	98	49	6.0‐6.2	6.0‐6.2	PRON
eurjchem-1369	98	50	(	(	PUNCT
eurjchem-1369	98	51	s	s	PROPN
eurjchem-1369	98	52	,	,	PUNCT
eurjchem-1369	98	53	3h	3h	NUM
eurjchem-1369	98	54	,	,	PUNCT
eurjchem-1369	98	55	nh2	nh2	PROPN
eurjchem-1369	98	56	+	+	PROPN
eurjchem-1369	98	57	ar‐h	ar‐h	PROPN
eurjchem-1369	98	58	)	)	PUNCT
eurjchem-1369	98	59	,	,	PUNCT
eurjchem-1369	98	60	6.2	6.2	NUM
eurjchem-1369	98	61	(	(	PUNCT
eurjchem-1369	98	62	8.72	8.72	NUM
eurjchem-1369	98	63	(	(	PUNCT
eurjchem-1369	98	64	s	s	PROPN
eurjchem-1369	98	65	,	,	PUNCT
eurjchem-1369	98	66	1h	1h	NUM
eurjchem-1369	98	67	,	,	PUNCT
eurjchem-1369	98	68	nh	nh	PROPN
eurjchem-1369	98	69	)	)	PUNCT
eurjchem-1369	98	70	.	.	PUNCT
eurjchem-1369	99	1	ms	ms	NOUN
eurjchem-1369	99	2	(	(	PUNCT
eurjchem-1369	99	3	ei	ei	PROPN
eurjchem-1369	99	4	,	,	PUNCT
eurjchem-1369	99	5	m	m	PROPN
eurjchem-1369	99	6	/	/	SYM
eurjchem-1369	99	7	z	z	PROPN
eurjchem-1369	99	8	(	(	PUNCT
eurjchem-1369	99	9	%	%	NOUN
eurjchem-1369	99	10	)	)	PUNCT
eurjchem-1369	99	11	):	):	PUNCT
eurjchem-1369	99	12	277	277	NUM
eurjchem-1369	99	13	(	(	PUNCT
eurjchem-1369	99	14	m+	m+	NUM
eurjchem-1369	99	15	,	,	PUNCT
eurjchem-1369	99	16	35	35	NUM
eurjchem-1369	99	17	)	)	PUNCT
eurjchem-1369	99	18	.	.	PUNCT
eurjchem-1369	100	1	anal	anal	PROPN
eurjchem-1369	100	2	.	.	PUNCT
eurjchem-1369	100	3	calcd	calcd	NOUN
eurjchem-1369	100	4	.	.	PUNCT
eurjchem-1369	101	1	for	for	ADP
eurjchem-1369	101	2	c12h15n5o3	c12h15n5o3	PROPN
eurjchem-1369	101	3	:	:	PUNCT
eurjchem-1369	101	4	c	c	X
eurjchem-1369	101	5	,	,	PUNCT
eurjchem-1369	101	6	51.98	51.98	NUM
eurjchem-1369	101	7	;	;	PUNCT
eurjchem-1369	101	8	h	h	NOUN
eurjchem-1369	101	9	,	,	PUNCT
eurjchem-1369	101	10	5.45	5.45	NUM
eurjchem-1369	101	11	;	;	PUNCT
eurjchem-1369	101	12	n	n	CCONJ
eurjchem-1369	101	13	,	,	PUNCT
eurjchem-1369	101	14	25.26	25.26	NUM
eurjchem-1369	101	15	.	.	PUNCT
eurjchem-1369	101	16	found	find	VERB
eurjchem-1369	101	17	:	:	PUNCT
eurjchem-1369	102	1	c	c	X
eurjchem-1369	102	2	,	,	PUNCT
eurjchem-1369	102	3	51.92	51.92	NUM
eurjchem-1369	102	4	;	;	PUNCT
eurjchem-1369	102	5	h	h	NOUN
eurjchem-1369	102	6	,	,	PUNCT
eurjchem-1369	102	7	5.46	5.46	NUM
eurjchem-1369	102	8	;	;	PUNCT
eurjchem-1369	102	9	n	n	CCONJ
eurjchem-1369	102	10	,	,	PUNCT
eurjchem-1369	102	11	25.46	25.46	NUM
eurjchem-1369	102	12	%	%	NOUN
eurjchem-1369	102	13	.	.	PUNCT
eurjchem-1369	103	1	5‐methyl‐7‐oxo‐2‐ureido‐6	5‐methyl‐7‐oxo‐2‐ureido‐6	NUM
eurjchem-1369	103	2	,	,	PUNCT
eurjchem-1369	103	3	7‐dihydro‐pyrazolo[1,5‐a]pyrimi	7‐dihydro‐pyrazolo[1,5‐a]pyrimi	PROPN
eurjchem-1369	103	4	dine‐3‐carboxylic	dine‐3‐carboxylic	NUM
eurjchem-1369	103	5	acid	acid	ADJ
eurjchem-1369	103	6	ethyl	ethyl	NOUN
eurjchem-1369	103	7	ester	ester	NOUN
eurjchem-1369	103	8	(	(	PUNCT
eurjchem-1369	103	9	6a	6a	NOUN
eurjchem-1369	103	10	):	):	PUNCT
eurjchem-1369	103	11	color	color	NOUN
eurjchem-1369	103	12	:	:	PUNCT
eurjchem-1369	103	13	buff	buff	PROPN
eurjchem-1369	103	14	crystals	crystal	NOUN
eurjchem-1369	103	15	.	.	PUNCT
eurjchem-1369	104	1	yield	yield	NOUN
eurjchem-1369	104	2	:	:	PUNCT
eurjchem-1369	104	3	65	65	NUM
eurjchem-1369	104	4	%	%	NOUN
eurjchem-1369	104	5	.	.	PUNCT
eurjchem-1369	105	1	m.p	m.p	PROPN
eurjchem-1369	105	2	.	.	PROPN
eurjchem-1369	105	3	:	:	PUNCT
eurjchem-1369	106	1	267‐269	267‐269	NUM
eurjchem-1369	106	2	°	°	ADP
eurjchem-1369	106	3	c	c	PROPN
eurjchem-1369	106	4	.	.	PUNCT
eurjchem-1369	107	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	107	2	(	(	PUNCT
eurjchem-1369	107	3	kbr	kbr	PROPN
eurjchem-1369	107	4	,	,	PUNCT
eurjchem-1369	107	5			PROPN
eurjchem-1369	107	6	,	,	PUNCT
eurjchem-1369	107	7	cm‐1	cm‐1	PROPN
eurjchem-1369	107	8	):	):	PUNCT
eurjchem-1369	107	9	3304‐3477	3304‐3477	PROPN
eurjchem-1369	107	10	(	(	PUNCT
eurjchem-1369	107	11	nh2	nh2	PROPN
eurjchem-1369	107	12	)	)	PUNCT
eurjchem-1369	107	13	,	,	PUNCT
eurjchem-1369	107	14	3294	3294	NUM
eurjchem-1369	107	15	(	(	PUNCT
eurjchem-1369	107	16	nh	nh	NOUN
eurjchem-1369	107	17	)	)	PUNCT
eurjchem-1369	107	18	,	,	PUNCT
eurjchem-1369	107	19	1693	1693	NUM
eurjchem-1369	107	20	,	,	PUNCT
eurjchem-1369	107	21	1640	1640	NUM
eurjchem-1369	107	22	(	(	PUNCT
eurjchem-1369	107	23	c	c	X
eurjchem-1369	107	24	=	=	SYM
eurjchem-1369	107	25	o	o	NOUN
eurjchem-1369	107	26	's	's	PART
eurjchem-1369	107	27	)	)	PUNCT
eurjchem-1369	107	28	.	.	PUNCT
eurjchem-1369	108	1	1h	1h	NUM
eurjchem-1369	108	2	nmr	nmr	NOUN
eurjchem-1369	108	3	(	(	PUNCT
eurjchem-1369	108	4	250	250	NUM
eurjchem-1369	108	5	mhz	mhz	NOUN
eurjchem-1369	108	6	,	,	PUNCT
eurjchem-1369	108	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	108	8	,	,	PUNCT
eurjchem-1369	108	9	δ	δ	PROPN
eurjchem-1369	108	10	,	,	PUNCT
eurjchem-1369	108	11	ppm	ppm	NUM
eurjchem-1369	108	12	):	):	PUNCT
eurjchem-1369	108	13	1.28‐1.32	1.28‐1.32	NUM
eurjchem-1369	108	14	(	(	PUNCT
eurjchem-1369	108	15	t	t	PROPN
eurjchem-1369	108	16	,	,	PUNCT
eurjchem-1369	108	17	3h	3h	NUM
eurjchem-1369	108	18	,	,	PUNCT
eurjchem-1369	108	19	ch3	ch3	PROPN
eurjchem-1369	108	20	)	)	PUNCT
eurjchem-1369	108	21	,	,	PUNCT
eurjchem-1369	108	22	2.32	2.32	NUM
eurjchem-1369	108	23	(	(	PUNCT
eurjchem-1369	108	24	s	s	PROPN
eurjchem-1369	108	25	,	,	PUNCT
eurjchem-1369	108	26	3h	3h	NUM
eurjchem-1369	108	27	,	,	PUNCT
eurjchem-1369	108	28	ch3	ch3	PROPN
eurjchem-1369	108	29	)	)	PUNCT
eurjchem-1369	108	30	,	,	PUNCT
eurjchem-1369	108	31	4.24‐4.33	4.24‐4.33	PROPN
eurjchem-1369	108	32	(	(	PUNCT
eurjchem-1369	108	33	q	q	NOUN
eurjchem-1369	108	34	,	,	PUNCT
eurjchem-1369	108	35	2h	2h	NUM
eurjchem-1369	108	36	,	,	PUNCT
eurjchem-1369	108	37	ch2	ch2	PROPN
eurjchem-1369	108	38	)	)	PUNCT
eurjchem-1369	108	39	,	,	PUNCT
eurjchem-1369	108	40	5.88	5.88	NUM
eurjchem-1369	108	41	(	(	PUNCT
eurjchem-1369	108	42	s	s	PROPN
eurjchem-1369	108	43	,	,	PUNCT
eurjchem-1369	108	44	2h	2h	NUM
eurjchem-1369	108	45	,	,	PUNCT
eurjchem-1369	108	46	ch2	ch2	PROPN
eurjchem-1369	108	47	)	)	PUNCT
eurjchem-1369	108	48	,	,	PUNCT
eurjchem-1369	108	49	5.95	5.95	NUM
eurjchem-1369	108	50	(	(	PUNCT
eurjchem-1369	108	51	s	s	PROPN
eurjchem-1369	108	52	,	,	PUNCT
eurjchem-1369	108	53	2h	2h	NUM
eurjchem-1369	108	54	,	,	PUNCT
eurjchem-1369	108	55	nh2	nh2	PROPN
eurjchem-1369	108	56	)	)	PUNCT
eurjchem-1369	108	57	,	,	PUNCT
eurjchem-1369	108	58	11.23	11.23	NUM
eurjchem-1369	108	59	(	(	PUNCT
eurjchem-1369	108	60	s	s	PROPN
eurjchem-1369	108	61	,	,	PUNCT
eurjchem-1369	108	62	1h	1h	NUM
eurjchem-1369	108	63	,	,	PUNCT
eurjchem-1369	108	64	nh	nh	PROPN
eurjchem-1369	108	65	)	)	PUNCT
eurjchem-1369	108	66	.	.	PUNCT
eurjchem-1369	109	1	13c	13c	NOUN
eurjchem-1369	109	2	nmr	nmr	NOUN
eurjchem-1369	109	3	(	(	PUNCT
eurjchem-1369	109	4	75	75	NUM
eurjchem-1369	109	5	mhz	mhz	NOUN
eurjchem-1369	109	6	,	,	PUNCT
eurjchem-1369	109	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	109	8	,	,	PUNCT
eurjchem-1369	109	9	δ	δ	PROPN
eurjchem-1369	109	10	,	,	PUNCT
eurjchem-1369	109	11	ppm	ppm	NUM
eurjchem-1369	109	12	):	):	PUNCT
eurjchem-1369	109	13	14.70	14.70	NUM
eurjchem-1369	109	14	(	(	PUNCT
eurjchem-1369	109	15	1c	1c	NOUN
eurjchem-1369	109	16	,	,	PUNCT
eurjchem-1369	109	17	ch3	ch3	PROPN
eurjchem-1369	109	18	)	)	PUNCT
eurjchem-1369	109	19	,	,	PUNCT
eurjchem-1369	109	20	19.06	19.06	NUM
eurjchem-1369	109	21	(	(	PUNCT
eurjchem-1369	109	22	1c	1c	X
eurjchem-1369	109	23	,	,	PUNCT
eurjchem-1369	109	24	ch3	ch3	PROPN
eurjchem-1369	109	25	)	)	PUNCT
eurjchem-1369	109	26	,	,	PUNCT
eurjchem-1369	109	27	59.65	59.65	NUM
eurjchem-1369	109	28	(	(	PUNCT
eurjchem-1369	109	29	1c	1c	NOUN
eurjchem-1369	109	30	,	,	PUNCT
eurjchem-1369	109	31	ch2	ch2	PROPN
eurjchem-1369	109	32	)	)	PUNCT
eurjchem-1369	109	33	,	,	PUNCT
eurjchem-1369	109	34	83.56	83.56	NUM
eurjchem-1369	109	35	(	(	PUNCT
eurjchem-1369	109	36	1c	1c	NOUN
eurjchem-1369	109	37	,	,	PUNCT
eurjchem-1369	109	38	ch2co	ch2co	NOUN
eurjchem-1369	109	39	)	)	PUNCT
eurjchem-1369	109	40	,	,	PUNCT
eurjchem-1369	109	41	99.65	99.65	NUM
eurjchem-1369	109	42	(	(	PUNCT
eurjchem-1369	109	43	1c	1c	NOUN
eurjchem-1369	109	44	,	,	PUNCT
eurjchem-1369	109	45	=	=	NOUN
eurjchem-1369	109	46	c‐ch3	c‐ch3	ADJ
eurjchem-1369	109	47	)	)	PUNCT
eurjchem-1369	109	48	,	,	PUNCT
eurjchem-1369	109	49	143	143	NUM
eurjchem-1369	109	50	(	(	PUNCT
eurjchem-1369	109	51	1c	1c	X
eurjchem-1369	109	52	,	,	PUNCT
eurjchem-1369	109	53	=	=	NOUN
eurjchem-1369	109	54	c‐n	c‐n	X
eurjchem-1369	109	55	)	)	PUNCT
eurjchem-1369	109	56	,	,	PUNCT
eurjchem-1369	109	57	144	144	NUM
eurjchem-1369	109	58	(	(	PUNCT
eurjchem-1369	109	59	1c	1c	X
eurjchem-1369	109	60	,	,	PUNCT
eurjchem-1369	109	61	n	n	CCONJ
eurjchem-1369	109	62	=	=	SYM
eurjchem-1369	109	63	c‐n	c‐n	NOUN
eurjchem-1369	109	64	)	)	PUNCT
eurjchem-1369	109	65	,	,	PUNCT
eurjchem-1369	109	66	149	149	NUM
eurjchem-1369	109	67	(	(	PUNCT
eurjchem-1369	109	68	1c	1c	NOUN
eurjchem-1369	109	69	,	,	PUNCT
eurjchem-1369	109	70	=	=	PRON
eurjchem-1369	109	71	c‐cooet	c‐cooet	NUM
eurjchem-1369	109	72	)	)	PUNCT
eurjchem-1369	109	73	,	,	PUNCT
eurjchem-1369	109	74	154	154	NUM
eurjchem-1369	109	75	(	(	PUNCT
eurjchem-1369	109	76	1c	1c	NOUN
eurjchem-1369	109	77	,	,	PUNCT
eurjchem-1369	109	78	conh2	conh2	PROPN
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eurjchem-1369	109	80	,	,	PUNCT
eurjchem-1369	109	81	157	157	NUM
eurjchem-1369	109	82	(	(	PUNCT
eurjchem-1369	109	83	1c	1c	NOUN
eurjchem-1369	109	84	,	,	PUNCT
eurjchem-1369	109	85	cooet	cooet	NOUN
eurjchem-1369	109	86	)	)	PUNCT
eurjchem-1369	109	87	,	,	PUNCT
eurjchem-1369	109	88	162.89	162.89	NUM
eurjchem-1369	109	89	(	(	PUNCT
eurjchem-1369	109	90	1c	1c	NOUN
eurjchem-1369	109	91	,	,	PUNCT
eurjchem-1369	109	92	c	c	NOUN
eurjchem-1369	109	93	=	=	NOUN
eurjchem-1369	109	94	o	o	NOUN
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eurjchem-1369	109	96	.	.	PUNCT
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eurjchem-1369	110	2	(	(	PUNCT
eurjchem-1369	110	3	ei	ei	PROPN
eurjchem-1369	110	4	,	,	PUNCT
eurjchem-1369	110	5	m	m	PROPN
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eurjchem-1369	110	7	z	z	PROPN
eurjchem-1369	110	8	(	(	PUNCT
eurjchem-1369	110	9	%	%	NOUN
eurjchem-1369	110	10	)	)	PUNCT
eurjchem-1369	110	11	):	):	PUNCT
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eurjchem-1369	110	13	(	(	PUNCT
eurjchem-1369	110	14	m+	m+	NUM
eurjchem-1369	110	15	,	,	PUNCT
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eurjchem-1369	110	17	)	)	PUNCT
eurjchem-1369	110	18	.	.	PUNCT
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eurjchem-1369	111	2	.	.	PUNCT
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eurjchem-1369	111	4	.	.	PUNCT
eurjchem-1369	112	1	for	for	ADP
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eurjchem-1369	112	5	,	,	PUNCT
eurjchem-1369	112	6	47.31	47.31	NUM
eurjchem-1369	112	7	;	;	PUNCT
eurjchem-1369	112	8	h	h	NOUN
eurjchem-1369	112	9	,	,	PUNCT
eurjchem-1369	112	10	4.69	4.69	NUM
eurjchem-1369	112	11	;	;	PUNCT
eurjchem-1369	112	12	n	n	CCONJ
eurjchem-1369	112	13	,	,	PUNCT
eurjchem-1369	112	14	25.08	25.08	NUM
eurjchem-1369	112	15	.	.	PUNCT
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eurjchem-1369	112	17	;	;	PUNCT
eurjchem-1369	112	18	c	c	X
eurjchem-1369	112	19	,	,	PUNCT
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eurjchem-1369	112	21	;	;	PUNCT
eurjchem-1369	113	1	h	h	NOUN
eurjchem-1369	113	2	,	,	PUNCT
eurjchem-1369	113	3	4.35	4.35	NUM
eurjchem-1369	113	4	;	;	PUNCT
eurjchem-1369	113	5	n	n	CCONJ
eurjchem-1369	113	6	,	,	PUNCT
eurjchem-1369	113	7	24.78	24.78	NUM
eurjchem-1369	113	8	%	%	NOUN
eurjchem-1369	113	9	.	.	PUNCT
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eurjchem-1369	114	2	,	,	PUNCT
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eurjchem-1369	114	4	zolo[1,5‐a]pyrimidine‐3‐carboxylic	zolo[1,5‐a]pyrimidine‐3‐carboxylic	PROPN
eurjchem-1369	114	5	acid	acid	PROPN
eurjchem-1369	114	6	ethyl	ethyl	PROPN
eurjchem-1369	114	7	ester	ester	NOUN
eurjchem-1369	114	8	(	(	PUNCT
eurjchem-1369	114	9	6b	6b	NOUN
eurjchem-1369	114	10	):	):	PUNCT
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eurjchem-1369	114	12	:	:	PUNCT
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eurjchem-1369	114	15	.	.	PUNCT
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eurjchem-1369	115	2	:	:	PUNCT
eurjchem-1369	115	3	46	46	NUM
eurjchem-1369	115	4	%	%	NOUN
eurjchem-1369	115	5	.	.	PUNCT
eurjchem-1369	116	1	m.p	m.p	PROPN
eurjchem-1369	116	2	.	.	PROPN
eurjchem-1369	116	3	:	:	PUNCT
eurjchem-1369	117	1	255‐257	255‐257	NOUN
eurjchem-1369	117	2	°	°	SYM
eurjchem-1369	117	3	c	c	NOUN
eurjchem-1369	117	4	.	.	PUNCT
eurjchem-1369	118	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	118	2	(	(	PUNCT
eurjchem-1369	118	3	kbr	kbr	PROPN
eurjchem-1369	118	4	,	,	PUNCT
eurjchem-1369	118	5			PROPN
eurjchem-1369	118	6	,	,	PUNCT
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eurjchem-1369	118	8	):	):	PUNCT
eurjchem-1369	118	9	3319‐3447	3319‐3447	NUM
eurjchem-1369	118	10	(	(	PUNCT
eurjchem-1369	118	11	nh2	nh2	PROPN
eurjchem-1369	118	12	)	)	PUNCT
eurjchem-1369	118	13	,	,	PUNCT
eurjchem-1369	118	14	3274	3274	NUM
eurjchem-1369	118	15	(	(	PUNCT
eurjchem-1369	118	16	nh	nh	NOUN
eurjchem-1369	118	17	)	)	PUNCT
eurjchem-1369	118	18	,	,	PUNCT
eurjchem-1369	118	19	1715	1715	NUM
eurjchem-1369	118	20	,	,	PUNCT
eurjchem-1369	118	21	1701	1701	NUM
eurjchem-1369	118	22	,	,	PUNCT
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eurjchem-1369	118	24	(	(	PUNCT
eurjchem-1369	118	25	c	c	X
eurjchem-1369	118	26	=	=	SYM
eurjchem-1369	118	27	o	o	NOUN
eurjchem-1369	118	28	's	's	PART
eurjchem-1369	118	29	)	)	PUNCT
eurjchem-1369	118	30	.	.	PUNCT
eurjchem-1369	119	1	1h	1h	NUM
eurjchem-1369	119	2	nmr	nmr	NOUN
eurjchem-1369	119	3	(	(	PUNCT
eurjchem-1369	119	4	250	250	NUM
eurjchem-1369	119	5	mhz	mhz	NOUN
eurjchem-1369	119	6	,	,	PUNCT
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eurjchem-1369	119	8	,	,	PUNCT
eurjchem-1369	119	9	δ	δ	PROPN
eurjchem-1369	119	10	,	,	PUNCT
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eurjchem-1369	119	12	):	):	PUNCT
eurjchem-1369	119	13	1.15	1.15	NUM
eurjchem-1369	119	14	(	(	PUNCT
eurjchem-1369	119	15	t	t	PROPN
eurjchem-1369	119	16	,	,	PUNCT
eurjchem-1369	119	17	3h	3h	NUM
eurjchem-1369	119	18	,	,	PUNCT
eurjchem-1369	119	19	ch3	ch3	PROPN
eurjchem-1369	119	20	)	)	PUNCT
eurjchem-1369	119	21	,	,	PUNCT
eurjchem-1369	119	22	1.22	1.22	NUM
eurjchem-1369	119	23	(	(	PUNCT
eurjchem-1369	119	24	t	t	PROPN
eurjchem-1369	119	25	,	,	PUNCT
eurjchem-1369	119	26	3h	3h	NUM
eurjchem-1369	119	27	,	,	PUNCT
eurjchem-1369	119	28	ch3	ch3	PROPN
eurjchem-1369	119	29	)	)	PUNCT
eurjchem-1369	119	30	,	,	PUNCT
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eurjchem-1369	119	32	(	(	PUNCT
eurjchem-1369	119	33	s	s	NOUN
eurjchem-1369	119	34	,	,	PUNCT
eurjchem-1369	119	35	2h	2h	NUM
eurjchem-1369	119	36	,	,	PUNCT
eurjchem-1369	119	37	ch2	ch2	PROPN
eurjchem-1369	119	38	)	)	PUNCT
eurjchem-1369	119	39	,	,	PUNCT
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eurjchem-1369	119	41	(	(	PUNCT
eurjchem-1369	119	42	q	q	NOUN
eurjchem-1369	119	43	,	,	PUNCT
eurjchem-1369	119	44	2h	2h	NUM
eurjchem-1369	119	45	,	,	PUNCT
eurjchem-1369	119	46	‐ch2	‐ch2	NUM
eurjchem-1369	119	47	)	)	PUNCT
eurjchem-1369	119	48	,	,	PUNCT
eurjchem-1369	119	49	4.25‐4.33	4.25‐4.33	PROPN
eurjchem-1369	119	50	(	(	PUNCT
eurjchem-1369	119	51	q	q	X
eurjchem-1369	119	52	,	,	PUNCT
eurjchem-1369	119	53	2h	2h	NUM
eurjchem-1369	119	54	,	,	PUNCT
eurjchem-1369	119	55	ch2	ch2	PROPN
eurjchem-1369	119	56	)	)	PUNCT
eurjchem-1369	119	57	,	,	PUNCT
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eurjchem-1369	119	59	(	(	PUNCT
eurjchem-1369	119	60	s	s	PROPN
eurjchem-1369	119	61	,	,	PUNCT
eurjchem-1369	119	62	2h	2h	NUM
eurjchem-1369	119	63	,	,	PUNCT
eurjchem-1369	119	64	ch2	ch2	PROPN
eurjchem-1369	119	65	)	)	PUNCT
eurjchem-1369	119	66	,	,	PUNCT
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eurjchem-1369	119	69	br.s	br.s	PROPN
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eurjchem-1369	119	72	,	,	PUNCT
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eurjchem-1369	119	74	)	)	PUNCT
eurjchem-1369	119	75	,	,	PUNCT
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eurjchem-1369	119	80	1h	1h	NUM
eurjchem-1369	119	81	,	,	PUNCT
eurjchem-1369	119	82	nh	nh	PROPN
eurjchem-1369	119	83	)	)	PUNCT
eurjchem-1369	119	84	.	.	PUNCT
eurjchem-1369	120	1	13c	13c	NOUN
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eurjchem-1369	120	3	(	(	PUNCT
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eurjchem-1369	120	6	,	,	PUNCT
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eurjchem-1369	120	8	,	,	PUNCT
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eurjchem-1369	120	10	,	,	PUNCT
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eurjchem-1369	120	12	):	):	PUNCT
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eurjchem-1369	120	14	(	(	PUNCT
eurjchem-1369	120	15	1c	1c	NOUN
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eurjchem-1369	120	17	ch3	ch3	PROPN
eurjchem-1369	120	18	)	)	PUNCT
eurjchem-1369	120	19	,	,	PUNCT
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eurjchem-1369	120	22	1c	1c	X
eurjchem-1369	120	23	,	,	PUNCT
eurjchem-1369	120	24	ch3	ch3	PROPN
eurjchem-1369	120	25	)	)	PUNCT
eurjchem-1369	120	26	,	,	PUNCT
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eurjchem-1369	120	29	1c	1c	NOUN
eurjchem-1369	120	30	,	,	PUNCT
eurjchem-1369	120	31	ch2	ch2	PROPN
eurjchem-1369	120	32	)	)	PUNCT
eurjchem-1369	120	33	,	,	PUNCT
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eurjchem-1369	120	35	(	(	PUNCT
eurjchem-1369	120	36	1c	1c	NOUN
eurjchem-1369	120	37	,	,	PUNCT
eurjchem-1369	120	38	ch2	ch2	PROPN
eurjchem-1369	120	39	)	)	PUNCT
eurjchem-1369	120	40	,	,	PUNCT
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eurjchem-1369	120	42	(	(	PUNCT
eurjchem-1369	120	43	1c	1c	NUM
eurjchem-1369	120	44	,	,	PUNCT
eurjchem-1369	120	45	n	n	CCONJ
eurjchem-1369	120	46	=	=	NOUN
eurjchem-1369	120	47	c‐	c‐	NOUN
eurjchem-1369	120	48	)	)	PUNCT
eurjchem-1369	120	49	,	,	PUNCT
eurjchem-1369	120	50	103	103	NUM
eurjchem-1369	120	51	(	(	PUNCT
eurjchem-1369	120	52	1c	1c	X
eurjchem-1369	120	53	,	,	PUNCT
eurjchem-1369	120	54	ch2	ch2	PROPN
eurjchem-1369	120	55	co	co	NOUN
eurjchem-1369	120	56	)	)	PUNCT
eurjchem-1369	120	57	,	,	PUNCT
eurjchem-1369	120	58	104	104	NUM
eurjchem-1369	120	59	(	(	PUNCT
eurjchem-1369	120	60	1c	1c	X
eurjchem-1369	120	61	,	,	PUNCT
eurjchem-1369	120	62	ch2co	ch2co	NOUN
eurjchem-1369	120	63	)	)	PUNCT
eurjchem-1369	120	64	,	,	PUNCT
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eurjchem-1369	120	67	1c	1c	NOUN
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eurjchem-1369	120	70	c‐n	c‐n	X
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eurjchem-1369	120	72	,	,	PUNCT
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eurjchem-1369	120	74	(	(	PUNCT
eurjchem-1369	120	75	1c	1c	NOUN
eurjchem-1369	120	76	,	,	PUNCT
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eurjchem-1369	120	78	=	=	SYM
eurjchem-1369	120	79	n	n	CCONJ
eurjchem-1369	120	80	)	)	PUNCT
eurjchem-1369	120	81	,	,	PUNCT
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eurjchem-1369	120	83	(	(	PUNCT
eurjchem-1369	120	84	1c	1c	NOUN
eurjchem-1369	120	85	,	,	PUNCT
eurjchem-1369	120	86	=	=	PRON
eurjchem-1369	120	87	c‐cooet	c‐cooet	NUM
eurjchem-1369	120	88	)	)	PUNCT
eurjchem-1369	120	89	,	,	PUNCT
eurjchem-1369	120	90	153.74	153.74	NUM
eurjchem-1369	120	91	(	(	PUNCT
eurjchem-1369	120	92	1c	1c	NOUN
eurjchem-1369	120	93	,	,	PUNCT
eurjchem-1369	120	94	conh2	conh2	PROPN
eurjchem-1369	120	95	)	)	PUNCT
eurjchem-1369	120	96	,	,	PUNCT
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eurjchem-1369	120	106	(	(	PUNCT
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eurjchem-1369	120	109	(	(	PUNCT
eurjchem-1369	120	110	2016	2016	NUM
eurjchem-1369	120	111	)	)	PUNCT
eurjchem-1369	120	112	107‐114	107‐114	NUM
eurjchem-1369	120	113	109	109	NUM
eurjchem-1369	120	114	scheme	scheme	NOUN
eurjchem-1369	120	115	2	2	NUM
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eurjchem-1369	120	117	(	(	PUNCT
eurjchem-1369	120	118	1c	1c	NOUN
eurjchem-1369	120	119	,	,	PUNCT
eurjchem-1369	120	120	cooet	cooet	NOUN
eurjchem-1369	120	121	)	)	PUNCT
eurjchem-1369	120	122	,	,	PUNCT
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eurjchem-1369	120	124	(	(	PUNCT
eurjchem-1369	120	125	1c	1c	NOUN
eurjchem-1369	120	126	,	,	PUNCT
eurjchem-1369	120	127	cooet	cooet	NOUN
eurjchem-1369	120	128	)	)	PUNCT
eurjchem-1369	120	129	,	,	PUNCT
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eurjchem-1369	120	131	(	(	PUNCT
eurjchem-1369	120	132	1c	1c	NOUN
eurjchem-1369	120	133	,	,	PUNCT
eurjchem-1369	120	134	c	c	NOUN
eurjchem-1369	120	135	=	=	NOUN
eurjchem-1369	120	136	o	o	NOUN
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eurjchem-1369	120	138	.	.	PUNCT
eurjchem-1369	121	1	ms	ms	NOUN
eurjchem-1369	121	2	(	(	PUNCT
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eurjchem-1369	121	4	,	,	PUNCT
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eurjchem-1369	121	7	z	z	PROPN
eurjchem-1369	121	8	(	(	PUNCT
eurjchem-1369	121	9	%	%	NOUN
eurjchem-1369	121	10	)	)	PUNCT
eurjchem-1369	121	11	):	):	PUNCT
eurjchem-1369	121	12	351	351	NUM
eurjchem-1369	121	13	(	(	PUNCT
eurjchem-1369	121	14	m+	m+	NUM
eurjchem-1369	121	15	,	,	PUNCT
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eurjchem-1369	121	17	)	)	PUNCT
eurjchem-1369	121	18	.	.	PUNCT
eurjchem-1369	122	1	anal	anal	PROPN
eurjchem-1369	122	2	.	.	PUNCT
eurjchem-1369	122	3	calcd	calcd	NOUN
eurjchem-1369	122	4	.	.	PUNCT
eurjchem-1369	123	1	for	for	SCONJ
eurjchem-1369	123	2	c14h17n5o6	c14h17n5o6	ADJ
eurjchem-1369	123	3	:	:	PUNCT
eurjchem-1369	123	4	c	c	X
eurjchem-1369	123	5	,	,	PUNCT
eurjchem-1369	123	6	47.86	47.86	NUM
eurjchem-1369	123	7	;	;	PUNCT
eurjchem-1369	123	8	h	h	NOUN
eurjchem-1369	123	9	,	,	PUNCT
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eurjchem-1369	123	11	;	;	PUNCT
eurjchem-1369	123	12	n	n	CCONJ
eurjchem-1369	123	13	,	,	PUNCT
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eurjchem-1369	123	15	.	.	PUNCT
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eurjchem-1369	123	17	:	:	PUNCT
eurjchem-1369	124	1	c	c	X
eurjchem-1369	124	2	,	,	PUNCT
eurjchem-1369	124	3	47.87	47.87	NUM
eurjchem-1369	124	4	;	;	PUNCT
eurjchem-1369	124	5	h	h	NOUN
eurjchem-1369	124	6	,	,	PUNCT
eurjchem-1369	124	7	4.96	4.96	NUM
eurjchem-1369	124	8	;	;	PUNCT
eurjchem-1369	124	9	n	n	CCONJ
eurjchem-1369	124	10	,	,	PUNCT
eurjchem-1369	124	11	19.50	19.50	NUM
eurjchem-1369	124	12	%	%	NOUN
eurjchem-1369	124	13	.	.	PUNCT
eurjchem-1369	125	1	2.2.4	2.2.4	X
eurjchem-1369	125	2	.	.	X
eurjchem-1369	125	3	synthesis	synthesis	NOUN
eurjchem-1369	125	4	of	of	ADP
eurjchem-1369	125	5	5‐amino‐7‐(3‐benzyloxy‐phenyl)‐6‐cyano‐	5‐amino‐7‐(3‐benzyloxy‐phenyl)‐6‐cyano‐	ADJ
eurjchem-1369	125	6	2‐ureido‐pyrazolo[1,5‐a]pyrimidine‐3‐carboxylic	2‐ureido‐pyrazolo[1,5‐a]pyrimidine‐3‐carboxylic	PROPN
eurjchem-1369	125	7	acid	acid	NOUN
eurjchem-1369	125	8	ethyl	ethyl	NOUN
eurjchem-1369	125	9	ester	ester	NOUN
eurjchem-1369	125	10	(	(	PUNCT
eurjchem-1369	125	11	7	7	NUM
eurjchem-1369	125	12	)	)	PUNCT
eurjchem-1369	125	13	a	a	DET
eurjchem-1369	125	14	solution	solution	NOUN
eurjchem-1369	125	15	of	of	ADP
eurjchem-1369	125	16	compound	compound	NOUN
eurjchem-1369	125	17	4a	4a	NOUN
eurjchem-1369	125	18	(	(	PUNCT
eurjchem-1369	125	19	2.13	2.13	NUM
eurjchem-1369	125	20	g	g	NOUN
eurjchem-1369	125	21	,	,	PUNCT
eurjchem-1369	125	22	0.01	0.01	NUM
eurjchem-1369	125	23	mole	mole	NOUN
eurjchem-1369	125	24	)	)	PUNCT
eurjchem-1369	125	25	and	and	CCONJ
eurjchem-1369	125	26	2‐(3‐	2‐(3‐	NUM
eurjchem-1369	126	1	benzyloxybenzyliden)malononitrile	benzyloxybenzyliden)malononitrile	NOUN
eurjchem-1369	126	2	(	(	PUNCT
eurjchem-1369	126	3	2.6	2.6	NUM
eurjchem-1369	126	4	g	g	NOUN
eurjchem-1369	126	5	,	,	PUNCT
eurjchem-1369	126	6	0.01	0.01	NUM
eurjchem-1369	126	7	mole	mole	NOUN
eurjchem-1369	126	8	)	)	PUNCT
eurjchem-1369	126	9	in	in	ADP
eurjchem-1369	126	10	pyridine	pyridine	NOUN
eurjchem-1369	126	11	(	(	PUNCT
eurjchem-1369	126	12	20	20	NUM
eurjchem-1369	126	13	ml	ml	NOUN
eurjchem-1369	126	14	)	)	PUNCT
eurjchem-1369	126	15	was	be	AUX
eurjchem-1369	126	16	heated	heat	VERB
eurjchem-1369	126	17	under	under	ADP
eurjchem-1369	126	18	reflux	reflux	NOUN
eurjchem-1369	126	19	for	for	ADP
eurjchem-1369	126	20	2	2	NUM
eurjchem-1369	126	21	h.	h.	NOUN
eurjchem-1369	126	22	the	the	DET
eurjchem-1369	126	23	solvent	solvent	NOUN
eurjchem-1369	126	24	was	be	AUX
eurjchem-1369	126	25	then	then	ADV
eurjchem-1369	126	26	evaporated	evaporate	VERB
eurjchem-1369	126	27	in	in	ADP
eurjchem-1369	126	28	vacuum	vacuum	NOUN
eurjchem-1369	126	29	,	,	PUNCT
eurjchem-1369	126	30	and	and	CCONJ
eurjchem-1369	126	31	the	the	DET
eurjchem-1369	126	32	remaining	remain	VERB
eurjchem-1369	126	33	solid	solid	ADJ
eurjchem-1369	126	34	product	product	NOUN
eurjchem-1369	126	35	was	be	AUX
eurjchem-1369	126	36	crystallized	crystallize	VERB
eurjchem-1369	126	37	from	from	ADP
eurjchem-1369	126	38	methanol	methanol	NOUN
eurjchem-1369	126	39	(	(	PUNCT
eurjchem-1369	126	40	scheme	scheme	NOUN
eurjchem-1369	126	41	2	2	NUM
eurjchem-1369	126	42	)	)	PUNCT
eurjchem-1369	126	43	.	.	PUNCT
eurjchem-1369	127	1	color	color	NOUN
eurjchem-1369	127	2	:	:	PUNCT
eurjchem-1369	127	3	yellow	yellow	ADJ
eurjchem-1369	127	4	crystals	crystal	NOUN
eurjchem-1369	127	5	.	.	PUNCT
eurjchem-1369	128	1	yield	yield	NOUN
eurjchem-1369	128	2	:	:	PUNCT
eurjchem-1369	128	3	56	56	NUM
eurjchem-1369	128	4	%	%	NOUN
eurjchem-1369	128	5	.	.	PUNCT
eurjchem-1369	129	1	m.p	m.p	PROPN
eurjchem-1369	129	2	.	.	PROPN
eurjchem-1369	129	3	:	:	PUNCT
eurjchem-1369	130	1	222‐224	222‐224	NUM
eurjchem-1369	130	2	°	°	SYM
eurjchem-1369	130	3	c	c	X
eurjchem-1369	130	4	.	.	PUNCT
eurjchem-1369	131	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	131	2	(	(	PUNCT
eurjchem-1369	131	3	kbr	kbr	PROPN
eurjchem-1369	131	4	,	,	PUNCT
eurjchem-1369	131	5			PROPN
eurjchem-1369	131	6	,	,	PUNCT
eurjchem-1369	131	7	cm‐1	cm‐1	PROPN
eurjchem-1369	131	8	):	):	PUNCT
eurjchem-1369	131	9	3357‐3479	3357‐3479	NUM
eurjchem-1369	131	10	(	(	PUNCT
eurjchem-1369	131	11	2nh2	2nh2	NUM
eurjchem-1369	131	12	)	)	PUNCT
eurjchem-1369	131	13	,	,	PUNCT
eurjchem-1369	131	14	3280	3280	NUM
eurjchem-1369	131	15	(	(	PUNCT
eurjchem-1369	131	16	nh	nh	NOUN
eurjchem-1369	131	17	)	)	PUNCT
eurjchem-1369	131	18	,	,	PUNCT
eurjchem-1369	131	19	2195	2195	NUM
eurjchem-1369	131	20	(	(	PUNCT
eurjchem-1369	131	21	cn	cn	PROPN
eurjchem-1369	131	22	)	)	PUNCT
eurjchem-1369	131	23	,	,	PUNCT
eurjchem-1369	131	24	1693	1693	NUM
eurjchem-1369	131	25	(	(	PUNCT
eurjchem-1369	131	26	c	c	NOUN
eurjchem-1369	131	27	=	=	NOUN
eurjchem-1369	131	28	o	o	NOUN
eurjchem-1369	131	29	)	)	PUNCT
eurjchem-1369	131	30	.	.	PUNCT
eurjchem-1369	132	1	1h	1h	NUM
eurjchem-1369	132	2	nmr	nmr	NOUN
eurjchem-1369	132	3	(	(	PUNCT
eurjchem-1369	132	4	250	250	NUM
eurjchem-1369	132	5	mhz	mhz	NOUN
eurjchem-1369	132	6	,	,	PUNCT
eurjchem-1369	132	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	132	8	,	,	PUNCT
eurjchem-1369	132	9	δ	δ	PROPN
eurjchem-1369	132	10	,	,	PUNCT
eurjchem-1369	132	11	ppm	ppm	NUM
eurjchem-1369	132	12	):	):	PUNCT
eurjchem-1369	132	13	1.25‐1.33	1.25‐1.33	NUM
eurjchem-1369	132	14	(	(	PUNCT
eurjchem-1369	132	15	t	t	PROPN
eurjchem-1369	132	16	,	,	PUNCT
eurjchem-1369	132	17	3h	3h	NUM
eurjchem-1369	132	18	,	,	PUNCT
eurjchem-1369	132	19	ch3	ch3	PROPN
eurjchem-1369	132	20	)	)	PUNCT
eurjchem-1369	132	21	,	,	PUNCT
eurjchem-1369	132	22	4.14‐4.23	4.14‐4.23	PROPN
eurjchem-1369	132	23	(	(	PUNCT
eurjchem-1369	132	24	q	q	NOUN
eurjchem-1369	132	25	,	,	PUNCT
eurjchem-1369	132	26	2h	2h	NUM
eurjchem-1369	132	27	,	,	PUNCT
eurjchem-1369	132	28	‐ch2	‐ch2	NUM
eurjchem-1369	132	29	)	)	PUNCT
eurjchem-1369	132	30	,	,	PUNCT
eurjchem-1369	132	31	5.20	5.20	NUM
eurjchem-1369	132	32	(	(	PUNCT
eurjchem-1369	132	33	s	s	PROPN
eurjchem-1369	132	34	,	,	PUNCT
eurjchem-1369	132	35	2h	2h	NUM
eurjchem-1369	132	36	,	,	PUNCT
eurjchem-1369	132	37	ch2	ch2	PROPN
eurjchem-1369	132	38	)	)	PUNCT
eurjchem-1369	132	39	,	,	PUNCT
eurjchem-1369	132	40	6.18	6.18	NUM
eurjchem-1369	132	41	(	(	PUNCT
eurjchem-1369	132	42	br.s	br.s	PROPN
eurjchem-1369	132	43	,	,	PUNCT
eurjchem-1369	132	44	2h	2h	NUM
eurjchem-1369	132	45	,	,	PUNCT
eurjchem-1369	132	46	nh2	nh2	PROPN
eurjchem-1369	132	47	)	)	PUNCT
eurjchem-1369	132	48	,	,	PUNCT
eurjchem-1369	132	49	6.4	6.4	NUM
eurjchem-1369	132	50	(	(	PUNCT
eurjchem-1369	132	51	br.s	br.s	PROPN
eurjchem-1369	132	52	,	,	PUNCT
eurjchem-1369	132	53	2h	2h	NUM
eurjchem-1369	132	54	,	,	PUNCT
eurjchem-1369	132	55	nh2	nh2	PROPN
eurjchem-1369	132	56	)	)	PUNCT
eurjchem-1369	132	57	,	,	PUNCT
eurjchem-1369	132	58	6.95‐7.33	6.95‐7.33	NUM
eurjchem-1369	132	59	(	(	PUNCT
eurjchem-1369	132	60	m	m	PROPN
eurjchem-1369	132	61	,	,	PUNCT
eurjchem-1369	132	62	9h	9h	NUM
eurjchem-1369	132	63	,	,	PUNCT
eurjchem-1369	132	64	ar‐h	ar‐h	NOUN
eurjchem-1369	132	65	)	)	PUNCT
eurjchem-1369	132	66	,	,	PUNCT
eurjchem-1369	132	67	7.15	7.15	NUM
eurjchem-1369	132	68	(	(	PUNCT
eurjchem-1369	132	69	s	s	PROPN
eurjchem-1369	132	70	,	,	PUNCT
eurjchem-1369	132	71	1h	1h	NUM
eurjchem-1369	132	72	,	,	PUNCT
eurjchem-1369	132	73	nh	nh	PROPN
eurjchem-1369	132	74	)	)	PUNCT
eurjchem-1369	132	75	.	.	PUNCT
eurjchem-1369	133	1	ms	ms	NOUN
eurjchem-1369	133	2	(	(	PUNCT
eurjchem-1369	133	3	ei	ei	PROPN
eurjchem-1369	133	4	,	,	PUNCT
eurjchem-1369	133	5	m	m	PROPN
eurjchem-1369	133	6	/	/	SYM
eurjchem-1369	133	7	z	z	PROPN
eurjchem-1369	133	8	(	(	PUNCT
eurjchem-1369	133	9	%	%	NOUN
eurjchem-1369	133	10	)	)	PUNCT
eurjchem-1369	133	11	):	):	PUNCT
eurjchem-1369	133	12	471	471	NUM
eurjchem-1369	133	13	(	(	PUNCT
eurjchem-1369	133	14	m+	m+	NUM
eurjchem-1369	133	15	,	,	PUNCT
eurjchem-1369	133	16	0.93	0.93	NUM
eurjchem-1369	133	17	)	)	PUNCT
eurjchem-1369	133	18	.	.	PUNCT
eurjchem-1369	134	1	anal	anal	PROPN
eurjchem-1369	134	2	.	.	PUNCT
eurjchem-1369	134	3	calcd	calcd	NOUN
eurjchem-1369	134	4	.	.	PUNCT
eurjchem-1369	135	1	for	for	ADP
eurjchem-1369	135	2	c24h21n7o4	c24h21n7o4	PROPN
eurjchem-1369	135	3	:	:	PUNCT
eurjchem-1369	135	4	c	c	NOUN
eurjchem-1369	135	5	,	,	PUNCT
eurjchem-1369	135	6	61.14	61.14	NUM
eurjchem-1369	135	7	;	;	PUNCT
eurjchem-1369	135	8	h	h	NOUN
eurjchem-1369	135	9	,	,	PUNCT
eurjchem-1369	135	10	4.49	4.49	NUM
eurjchem-1369	135	11	;	;	PUNCT
eurjchem-1369	135	12	n	n	CCONJ
eurjchem-1369	135	13	,	,	PUNCT
eurjchem-1369	135	14	20.80	20.80	NUM
eurjchem-1369	135	15	.	.	PUNCT
eurjchem-1369	135	16	found	find	VERB
eurjchem-1369	135	17	:	:	PUNCT
eurjchem-1369	136	1	c	c	X
eurjchem-1369	136	2	,	,	PUNCT
eurjchem-1369	136	3	61.34	61.34	NUM
eurjchem-1369	136	4	;	;	PUNCT
eurjchem-1369	136	5	h	h	NOUN
eurjchem-1369	136	6	,	,	PUNCT
eurjchem-1369	136	7	4.86	4.86	NUM
eurjchem-1369	136	8	;	;	PUNCT
eurjchem-1369	136	9	n	n	CCONJ
eurjchem-1369	136	10	,	,	PUNCT
eurjchem-1369	136	11	20.55	20.55	NUM
eurjchem-1369	136	12	%	%	NOUN
eurjchem-1369	136	13	.	.	PUNCT
eurjchem-1369	137	1	2.2.5	2.2.5	X
eurjchem-1369	137	2	.	.	PUNCT
eurjchem-1369	137	3	general	general	ADJ
eurjchem-1369	137	4	procedure	procedure	NOUN
eurjchem-1369	137	5	for	for	ADP
eurjchem-1369	137	6	the	the	DET
eurjchem-1369	137	7	synthesis	synthesis	NOUN
eurjchem-1369	137	8	of	of	ADP
eurjchem-1369	137	9	pyrazolo[1,5‐	pyrazolo[1,5‐	PROPN
eurjchem-1369	137	10	a]pyrimidines	a]pyrimidine	VERB
eurjchem-1369	137	11	9	9	NUM
eurjchem-1369	137	12	,	,	PUNCT
eurjchem-1369	137	13	10a‐c	10a‐c	NUM
eurjchem-1369	137	14	and	and	CCONJ
eurjchem-1369	137	15	11	11	NUM
eurjchem-1369	137	16	to	to	ADP
eurjchem-1369	137	17	a	a	DET
eurjchem-1369	137	18	solution	solution	NOUN
eurjchem-1369	137	19	of	of	ADP
eurjchem-1369	137	20	compound	compound	NOUN
eurjchem-1369	137	21	4a	4a	NOUN
eurjchem-1369	137	22	(	(	PUNCT
eurjchem-1369	137	23	2.13	2.13	NUM
eurjchem-1369	137	24	g	g	NOUN
eurjchem-1369	137	25	,	,	PUNCT
eurjchem-1369	137	26	0.01	0.01	NUM
eurjchem-1369	137	27	mole	mole	NOUN
eurjchem-1369	137	28	)	)	PUNCT
eurjchem-1369	137	29	in	in	ADP
eurjchem-1369	137	30	(	(	PUNCT
eurjchem-1369	137	31	10	10	NUM
eurjchem-1369	137	32	ml	ml	NOUN
eurjchem-1369	137	33	)	)	PUNCT
eurjchem-1369	137	34	dimethylformamide	dimethylformamide	NOUN
eurjchem-1369	137	35	and	and	CCONJ
eurjchem-1369	137	36	0.5	0.5	NUM
eurjchem-1369	137	37	g	g	NOUN
eurjchem-1369	137	38	potassium	potassium	NOUN
eurjchem-1369	137	39	carbonate	carbonate	NOUN
eurjchem-1369	137	40	,	,	PUNCT
eurjchem-1369	137	41	an	an	DET
eurjchem-1369	137	42	electrophilic	electrophilic	ADJ
eurjchem-1369	137	43	reagent	reagent	NOUN
eurjchem-1369	137	44	namely	namely	ADV
eurjchem-1369	137	45	,	,	PUNCT
eurjchem-1369	137	46	2‐cyano‐3,3‐bis(methylthio	2‐cyano‐3,3‐bis(methylthio	NUM
eurjchem-1369	137	47	)	)	PUNCT
eurjchem-1369	137	48	acrylonitrile	acrylonitrile	NOUN
eurjchem-1369	137	49	,	,	PUNCT
eurjchem-1369	137	50	3,3‐bis‐benzyl‐sulfanyl‐2‐cyano‐acrylic	3,3‐bis‐benzyl‐sulfanyl‐2‐cyano‐acrylic	NUM
eurjchem-1369	137	51	acid	acid	NOUN
eurjchem-1369	137	52	ethyl	ethyl	PROPN
eurjchem-1369	137	53	ester	ester	NOUN
eurjchem-1369	137	54	,	,	PUNCT
eurjchem-1369	137	55	2‐cyano‐3‐ethoxy‐carbonylmethylsulfanyl‐3‐phenyl‐amino	2‐cyano‐3‐ethoxy‐carbonylmethylsulfanyl‐3‐phenyl‐amino	PROPN
eurjchem-1369	137	56	acrylic	acrylic	NOUN
eurjchem-1369	137	57	acid	acid	NOUN
eurjchem-1369	137	58	ethyl	ethyl	PROPN
eurjchem-1369	137	59	ester	ester	NOUN
eurjchem-1369	137	60	,	,	PUNCT
eurjchem-1369	137	61	2‐cyano‐3‐methylsulfanyl‐3‐ureido‐	2‐cyano‐3‐methylsulfanyl‐3‐ureido‐	PROPN
eurjchem-1369	137	62	acrylic	acrylic	NOUN
eurjchem-1369	137	63	acid	acid	NOUN
eurjchem-1369	137	64	ethyl	ethyl	PROPN
eurjchem-1369	137	65	ester	ester	NOUN
eurjchem-1369	137	66	and	and	CCONJ
eurjchem-1369	137	67	ethyl‐2‐cyano‐3,3‐bis‐(methylthio	ethyl‐2‐cyano‐3,3‐bis‐(methylthio	ADJ
eurjchem-1369	137	68	)	)	PUNCT
eurjchem-1369	137	69	acrylate	acrylate	NOUN
eurjchem-1369	137	70	and	and	CCONJ
eurjchem-1369	137	71	2‐cyano‐3,3‐bis‐methylsulfanyl‐acryl	2‐cyano‐3,3‐bis‐methylsulfanyl‐acryl	NUM
eurjchem-1369	137	72	amide	amide	NOUN
eurjchem-1369	137	73	(	(	PUNCT
eurjchem-1369	137	74	0.01	0.01	NUM
eurjchem-1369	137	75	mole	mole	NOUN
eurjchem-1369	137	76	)	)	PUNCT
eurjchem-1369	137	77	was	be	AUX
eurjchem-1369	137	78	added	add	VERB
eurjchem-1369	137	79	.	.	PUNCT
eurjchem-1369	138	1	the	the	DET
eurjchem-1369	138	2	reaction	reaction	NOUN
eurjchem-1369	138	3	mixture	mixture	NOUN
eurjchem-1369	138	4	was	be	AUX
eurjchem-1369	138	5	stirred	stir	VERB
eurjchem-1369	138	6	at	at	ADP
eurjchem-1369	138	7	room	room	NOUN
eurjchem-1369	138	8	temperature	temperature	NOUN
eurjchem-1369	138	9	for	for	ADP
eurjchem-1369	138	10	the	the	DET
eurjchem-1369	138	11	appropriate	appropriate	ADJ
eurjchem-1369	138	12	time	time	NOUN
eurjchem-1369	138	13	(	(	PUNCT
eurjchem-1369	138	14	6‐14	6‐14	NUM
eurjchem-1369	138	15	h	h	NOUN
eurjchem-1369	138	16	)	)	PUNCT
eurjchem-1369	138	17	.	.	PUNCT
eurjchem-1369	139	1	after	after	ADP
eurjchem-1369	139	2	this	this	DET
eurjchem-1369	139	3	time	time	NOUN
eurjchem-1369	139	4	the	the	DET
eurjchem-1369	139	5	reaction	reaction	NOUN
eurjchem-1369	139	6	mixture	mixture	NOUN
eurjchem-1369	139	7	was	be	AUX
eurjchem-1369	139	8	acidified	acidify	VERB
eurjchem-1369	139	9	with	with	ADP
eurjchem-1369	139	10	10	10	NUM
eurjchem-1369	139	11	%	%	NOUN
eurjchem-1369	139	12	hydrochloric	hydrochloric	ADJ
eurjchem-1369	139	13	acid	acid	NOUN
eurjchem-1369	139	14	.	.	PUNCT
eurjchem-1369	140	1	the	the	DET
eurjchem-1369	140	2	precipitate	precipitate	NOUN
eurjchem-1369	140	3	that	that	PRON
eurjchem-1369	140	4	appeared	appear	VERB
eurjchem-1369	140	5	was	be	AUX
eurjchem-1369	140	6	collected	collect	VERB
eurjchem-1369	140	7	by	by	ADP
eurjchem-1369	140	8	filtration	filtration	NOUN
eurjchem-1369	140	9	and	and	CCONJ
eurjchem-1369	140	10	crystallized	crystallize	VERB
eurjchem-1369	140	11	from	from	ADP
eurjchem-1369	140	12	appropriate	appropriate	ADJ
eurjchem-1369	140	13	solvent	solvent	NOUN
eurjchem-1369	140	14	to	to	PART
eurjchem-1369	140	15	yield	yield	VERB
eurjchem-1369	140	16	compound	compound	NOUN
eurjchem-1369	140	17	9	9	NUM
eurjchem-1369	140	18	,	,	PUNCT
eurjchem-1369	140	19	10a‐c	10a‐c	NOUN
eurjchem-1369	140	20	and	and	CCONJ
eurjchem-1369	140	21	11	11	NUM
eurjchem-1369	140	22	,	,	PUNCT
eurjchem-1369	140	23	respectively	respectively	ADV
eurjchem-1369	140	24	(	(	PUNCT
eurjchem-1369	140	25	scheme	scheme	NOUN
eurjchem-1369	140	26	3	3	NUM
eurjchem-1369	140	27	)	)	PUNCT
eurjchem-1369	140	28	.	.	PUNCT
eurjchem-1369	141	1	7‐amino‐6‐cyano‐5‐methylsulfanyl‐2‐ureido‐pyrazolo[1	7‐amino‐6‐cyano‐5‐methylsulfanyl‐2‐ureido‐pyrazolo[1	NUM
eurjchem-1369	141	2	,	,	PUNCT
eurjchem-1369	141	3	5‐	5‐	PROPN
eurjchem-1369	141	4	a]pyrimidine‐3‐carboxylic	a]pyrimidine‐3‐carboxylic	PROPN
eurjchem-1369	141	5	acid	acid	PROPN
eurjchem-1369	141	6	ethyl	ethyl	PROPN
eurjchem-1369	141	7	ester	ester	NOUN
eurjchem-1369	141	8	(	(	PUNCT
eurjchem-1369	141	9	9	9	NUM
eurjchem-1369	141	10	):	):	PUNCT
eurjchem-1369	141	11	color	color	NOUN
eurjchem-1369	141	12	:	:	PUNCT
eurjchem-1369	141	13	yellow	yellow	ADJ
eurjchem-1369	141	14	crystals	crystal	NOUN
eurjchem-1369	141	15	.	.	PUNCT
eurjchem-1369	142	1	yield	yield	NOUN
eurjchem-1369	142	2	:	:	PUNCT
eurjchem-1369	142	3	62	62	NUM
eurjchem-1369	142	4	%	%	NOUN
eurjchem-1369	142	5	.	.	PUNCT
eurjchem-1369	143	1	m.p	m.p	PROPN
eurjchem-1369	143	2	.	.	PROPN
eurjchem-1369	143	3	:	:	PUNCT
eurjchem-1369	144	1	>	>	X
eurjchem-1369	144	2	360	360	NUM
eurjchem-1369	144	3	°	°	SYM
eurjchem-1369	144	4	c	c	X
eurjchem-1369	144	5	.	.	PUNCT
eurjchem-1369	145	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	145	2	(	(	PUNCT
eurjchem-1369	145	3	kbr	kbr	PROPN
eurjchem-1369	145	4	,	,	PUNCT
eurjchem-1369	145	5			PROPN
eurjchem-1369	145	6	,	,	PUNCT
eurjchem-1369	145	7	cm‐1	cm‐1	PROPN
eurjchem-1369	145	8	):	):	PUNCT
eurjchem-1369	145	9	3291‐	3291‐	NUM
eurjchem-1369	145	10	3412	3412	NUM
eurjchem-1369	145	11	(	(	PUNCT
eurjchem-1369	145	12	2nh2	2nh2	NUM
eurjchem-1369	145	13	)	)	PUNCT
eurjchem-1369	145	14	,	,	PUNCT
eurjchem-1369	145	15	3180	3180	NUM
eurjchem-1369	145	16	(	(	PUNCT
eurjchem-1369	145	17	nh	nh	NOUN
eurjchem-1369	145	18	)	)	PUNCT
eurjchem-1369	145	19	,	,	PUNCT
eurjchem-1369	145	20	2215	2215	NUM
eurjchem-1369	145	21	(	(	PUNCT
eurjchem-1369	145	22	cn	cn	PROPN
eurjchem-1369	145	23	)	)	PUNCT
eurjchem-1369	145	24	,	,	PUNCT
eurjchem-1369	145	25	1719‐1682	1719‐1682	NUM
eurjchem-1369	145	26	(	(	PUNCT
eurjchem-1369	145	27	c	c	X
eurjchem-1369	145	28	=	=	SYM
eurjchem-1369	145	29	o	o	NOUN
eurjchem-1369	145	30	's	's	PART
eurjchem-1369	145	31	)	)	PUNCT
eurjchem-1369	145	32	.	.	PUNCT
eurjchem-1369	146	1	1h	1h	NUM
eurjchem-1369	146	2	nmr	nmr	NOUN
eurjchem-1369	146	3	(	(	PUNCT
eurjchem-1369	146	4	250	250	NUM
eurjchem-1369	146	5	mhz	mhz	NOUN
eurjchem-1369	146	6	,	,	PUNCT
eurjchem-1369	146	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	146	8	,	,	PUNCT
eurjchem-1369	146	9	δ	δ	PROPN
eurjchem-1369	146	10	,	,	PUNCT
eurjchem-1369	146	11	ppm	ppm	NUM
eurjchem-1369	146	12	):	):	PUNCT
eurjchem-1369	146	13	1.23‐1.37	1.23‐1.37	PROPN
eurjchem-1369	146	14	(	(	PUNCT
eurjchem-1369	146	15	t	t	PROPN
eurjchem-1369	146	16	,	,	PUNCT
eurjchem-1369	146	17	3h	3h	NUM
eurjchem-1369	146	18	,	,	PUNCT
eurjchem-1369	146	19	ch3	ch3	PROPN
eurjchem-1369	146	20	)	)	PUNCT
eurjchem-1369	146	21	,	,	PUNCT
eurjchem-1369	146	22	2.71	2.71	NUM
eurjchem-1369	146	23	(	(	PUNCT
eurjchem-1369	146	24	s	s	PROPN
eurjchem-1369	146	25	,	,	PUNCT
eurjchem-1369	146	26	3h	3h	NUM
eurjchem-1369	146	27	,	,	PUNCT
eurjchem-1369	146	28	sch3	sch3	PROPN
eurjchem-1369	146	29	)	)	PUNCT
eurjchem-1369	146	30	,	,	PUNCT
eurjchem-1369	146	31	4.20‐4.27	4.20‐4.27	NUM
eurjchem-1369	146	32	(	(	PUNCT
eurjchem-1369	146	33	q	q	NOUN
eurjchem-1369	146	34	,	,	PUNCT
eurjchem-1369	146	35	2h	2h	NUM
eurjchem-1369	146	36	,	,	PUNCT
eurjchem-1369	146	37	‐ch2	‐ch2	NUM
eurjchem-1369	146	38	)	)	PUNCT
eurjchem-1369	146	39	,	,	PUNCT
eurjchem-1369	146	40	7.43	7.43	NUM
eurjchem-1369	146	41	(	(	PUNCT
eurjchem-1369	146	42	br.s	br.s	PROPN
eurjchem-1369	146	43	,	,	PUNCT
eurjchem-1369	146	44	2h	2h	NUM
eurjchem-1369	146	45	,	,	PUNCT
eurjchem-1369	146	46	nh2	nh2	PROPN
eurjchem-1369	146	47	)	)	PUNCT
eurjchem-1369	146	48	,	,	PUNCT
eurjchem-1369	146	49	8.74	8.74	NUM
eurjchem-1369	146	50	(	(	PUNCT
eurjchem-1369	146	51	br.s	br.s	PROPN
eurjchem-1369	146	52	,	,	PUNCT
eurjchem-1369	146	53	2h	2h	NUM
eurjchem-1369	146	54	,	,	PUNCT
eurjchem-1369	146	55	nh2	nh2	PROPN
eurjchem-1369	146	56	)	)	PUNCT
eurjchem-1369	146	57	,	,	PUNCT
eurjchem-1369	146	58	8.62	8.62	NUM
eurjchem-1369	146	59	(	(	PUNCT
eurjchem-1369	146	60	s	s	PROPN
eurjchem-1369	146	61	,	,	PUNCT
eurjchem-1369	146	62	1h	1h	NUM
eurjchem-1369	146	63	,	,	PUNCT
eurjchem-1369	146	64	nh	nh	PROPN
eurjchem-1369	146	65	)	)	PUNCT
eurjchem-1369	146	66	.	.	PUNCT
eurjchem-1369	147	1	13c	13c	NOUN
eurjchem-1369	147	2	nmr	nmr	NOUN
eurjchem-1369	147	3	(	(	PUNCT
eurjchem-1369	147	4	75	75	NUM
eurjchem-1369	147	5	mhz	mhz	NOUN
eurjchem-1369	147	6	,	,	PUNCT
eurjchem-1369	147	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	147	8	,	,	PUNCT
eurjchem-1369	147	9	δ	δ	PROPN
eurjchem-1369	147	10	,	,	PUNCT
eurjchem-1369	147	11	ppm	ppm	NUM
eurjchem-1369	147	12	):	):	PUNCT
eurjchem-1369	147	13	14.39	14.39	NUM
eurjchem-1369	147	14	(	(	PUNCT
eurjchem-1369	147	15	1c	1c	NOUN
eurjchem-1369	147	16	,	,	PUNCT
eurjchem-1369	147	17	ch3	ch3	PROPN
eurjchem-1369	147	18	)	)	PUNCT
eurjchem-1369	147	19	,	,	PUNCT
eurjchem-1369	147	20	16.32	16.32	NUM
eurjchem-1369	147	21	(	(	PUNCT
eurjchem-1369	147	22	1c	1c	NOUN
eurjchem-1369	147	23	,	,	PUNCT
eurjchem-1369	147	24	sch3	sch3	PROPN
eurjchem-1369	147	25	)	)	PUNCT
eurjchem-1369	147	26	,	,	PUNCT
eurjchem-1369	147	27	59.74	59.74	NUM
eurjchem-1369	147	28	(	(	PUNCT
eurjchem-1369	147	29	1c	1c	NOUN
eurjchem-1369	147	30	,	,	PUNCT
eurjchem-1369	147	31	ch2	ch2	PROPN
eurjchem-1369	147	32	)	)	PUNCT
eurjchem-1369	147	33	,	,	PUNCT
eurjchem-1369	147	34	84.23	84.23	NUM
eurjchem-1369	147	35	(	(	PUNCT
eurjchem-1369	147	36	1c	1c	NOUN
eurjchem-1369	147	37	,	,	PUNCT
eurjchem-1369	147	38	=	=	NOUN
eurjchem-1369	147	39	c‐n	c‐n	X
eurjchem-1369	147	40	)	)	PUNCT
eurjchem-1369	147	41	,	,	PUNCT
eurjchem-1369	147	42	84.5	84.5	NUM
eurjchem-1369	147	43	(	(	PUNCT
eurjchem-1369	147	44	1c	1c	X
eurjchem-1369	147	45	,	,	PUNCT
eurjchem-1369	147	46	n	n	CCONJ
eurjchem-1369	147	47	=	=	SYM
eurjchem-1369	147	48	c‐n	c‐n	NOUN
eurjchem-1369	147	49	)	)	PUNCT
eurjchem-1369	147	50	,	,	PUNCT
eurjchem-1369	147	51	114.12	114.12	NUM
eurjchem-1369	147	52	(	(	PUNCT
eurjchem-1369	147	53	1c	1c	NOUN
eurjchem-1369	147	54	,	,	PUNCT
eurjchem-1369	147	55	=	=	NOUN
eurjchem-1369	147	56	c‐nh2	c‐nh2	PROPN
eurjchem-1369	147	57	)	)	PUNCT
eurjchem-1369	147	58	,	,	PUNCT
eurjchem-1369	147	59	142.94	142.94	NUM
eurjchem-1369	147	60	(	(	PUNCT
eurjchem-1369	147	61	1c	1c	NOUN
eurjchem-1369	147	62	,	,	PUNCT
eurjchem-1369	147	63	=	=	NOUN
eurjchem-1369	147	64	c‐s	c‐s	NOUN
eurjchem-1369	147	65	)	)	PUNCT
eurjchem-1369	147	66	,	,	PUNCT
eurjchem-1369	147	67	153.15	153.15	NUM
eurjchem-1369	147	68	(	(	PUNCT
eurjchem-1369	147	69	1c	1c	NOUN
eurjchem-1369	147	70	,	,	PUNCT
eurjchem-1369	147	71	=	=	PRON
eurjchem-1369	147	72	c‐cooet	c‐cooet	NUM
eurjchem-1369	147	73	)	)	PUNCT
eurjchem-1369	147	74	,	,	PUNCT
eurjchem-1369	147	75	153.99	153.99	NUM
eurjchem-1369	147	76	(	(	PUNCT
eurjchem-1369	147	77	1c	1c	NOUN
eurjchem-1369	147	78	,	,	PUNCT
eurjchem-1369	147	79	=	=	NOUN
eurjchem-1369	147	80	c‐cn	c‐cn	NOUN
eurjchem-1369	147	81	)	)	PUNCT
eurjchem-1369	147	82	,	,	PUNCT
eurjchem-1369	147	83	154.46	154.46	NUM
eurjchem-1369	147	84	(	(	PUNCT
eurjchem-1369	147	85	1c	1c	NOUN
eurjchem-1369	147	86	,	,	PUNCT
eurjchem-1369	147	87	cn	cn	PROPN
eurjchem-1369	147	88	)	)	PUNCT
eurjchem-1369	147	89	,	,	PUNCT
eurjchem-1369	147	90	157.40	157.40	NUM
eurjchem-1369	147	91	(	(	PUNCT
eurjchem-1369	147	92	1c	1c	NOUN
eurjchem-1369	147	93	,	,	PUNCT
eurjchem-1369	147	94	conh2	conh2	PROPN
eurjchem-1369	147	95	)	)	PUNCT
eurjchem-1369	147	96	,	,	PUNCT
eurjchem-1369	147	97	163.62	163.62	NUM
eurjchem-1369	147	98	(	(	PUNCT
eurjchem-1369	147	99	1c	1c	NOUN
eurjchem-1369	147	100	,	,	PUNCT
eurjchem-1369	147	101	cooet	cooet	NOUN
eurjchem-1369	147	102	)	)	PUNCT
eurjchem-1369	147	103	.	.	PUNCT
eurjchem-1369	148	1	ms	ms	NOUN
eurjchem-1369	148	2	(	(	PUNCT
eurjchem-1369	148	3	ei	ei	PROPN
eurjchem-1369	148	4	,	,	PUNCT
eurjchem-1369	148	5	m	m	PROPN
eurjchem-1369	148	6	/	/	SYM
eurjchem-1369	148	7	z	z	PROPN
eurjchem-1369	148	8	(	(	PUNCT
eurjchem-1369	148	9	%	%	NOUN
eurjchem-1369	148	10	)	)	PUNCT
eurjchem-1369	148	11	):	):	PUNCT
eurjchem-1369	148	12	335	335	NUM
eurjchem-1369	148	13	(	(	PUNCT
eurjchem-1369	148	14	m+	m+	NUM
eurjchem-1369	148	15	,	,	PUNCT
eurjchem-1369	148	16	9.6	9.6	NUM
eurjchem-1369	148	17	)	)	PUNCT
eurjchem-1369	148	18	.	.	PUNCT
eurjchem-1369	149	1	anal	anal	PROPN
eurjchem-1369	149	2	.	.	PUNCT
eurjchem-1369	149	3	calcd	calcd	NOUN
eurjchem-1369	149	4	.	.	PUNCT
eurjchem-1369	150	1	for	for	ADP
eurjchem-1369	150	2	c12h13n7o3s	c12h13n7o3s	NUM
eurjchem-1369	150	3	:	:	PUNCT
eurjchem-1369	150	4	c	c	X
eurjchem-1369	150	5	,	,	PUNCT
eurjchem-1369	150	6	42.98	42.98	NUM
eurjchem-1369	150	7	;	;	PUNCT
eurjchem-1369	150	8	h	h	X
eurjchem-1369	150	9	,	,	PUNCT
eurjchem-1369	150	10	3.91	3.91	NUM
eurjchem-1369	150	11	;	;	PUNCT
eurjchem-1369	150	12	n	n	CCONJ
eurjchem-1369	150	13	,	,	PUNCT
eurjchem-1369	150	14	29.24	29.24	NUM
eurjchem-1369	150	15	.	.	PUNCT
eurjchem-1369	150	16	found	find	VERB
eurjchem-1369	150	17	;	;	PUNCT
eurjchem-1369	151	1	c	c	X
eurjchem-1369	151	2	,	,	PUNCT
eurjchem-1369	151	3	42.84	42.84	NUM
eurjchem-1369	151	4	;	;	PUNCT
eurjchem-1369	151	5	h	h	NOUN
eurjchem-1369	151	6	,	,	PUNCT
eurjchem-1369	151	7	3.92	3.92	NUM
eurjchem-1369	151	8	;	;	PUNCT
eurjchem-1369	151	9	n	n	CCONJ
eurjchem-1369	151	10	,	,	PUNCT
eurjchem-1369	151	11	29.57	29.57	NUM
eurjchem-1369	151	12	%	%	NOUN
eurjchem-1369	151	13	.	.	PUNCT
eurjchem-1369	152	1	5‐benzylsulfanyl‐6‐cyano‐7‐oxo‐2‐ureido‐4	5‐benzylsulfanyl‐6‐cyano‐7‐oxo‐2‐ureido‐4	NUM
eurjchem-1369	152	2	,	,	PUNCT
eurjchem-1369	152	3	7‐dihydro‐pyra	7‐dihydro‐pyra	NUM
eurjchem-1369	152	4	zolo[1,5‐a]pyrimidine‐3‐carboxylic	zolo[1,5‐a]pyrimidine‐3‐carboxylic	PROPN
eurjchem-1369	152	5	acid	acid	PROPN
eurjchem-1369	152	6	ethyl	ethyl	PROPN
eurjchem-1369	152	7	ester	ester	NOUN
eurjchem-1369	152	8	(	(	PUNCT
eurjchem-1369	152	9	10a	10a	NUM
eurjchem-1369	152	10	):	):	PUNCT
eurjchem-1369	152	11	color	color	NOUN
eurjchem-1369	152	12	:	:	PUNCT
eurjchem-1369	152	13	buff	buff	PROPN
eurjchem-1369	152	14	crystals	crystal	NOUN
eurjchem-1369	152	15	.	.	PUNCT
eurjchem-1369	153	1	yield	yield	NOUN
eurjchem-1369	153	2	:	:	PUNCT
eurjchem-1369	153	3	62	62	NUM
eurjchem-1369	153	4	%	%	NOUN
eurjchem-1369	153	5	.	.	PUNCT
eurjchem-1369	154	1	m.p	m.p	PROPN
eurjchem-1369	154	2	.	.	PROPN
eurjchem-1369	154	3	:	:	PUNCT
eurjchem-1369	155	1	322‐324	322‐324	NUM
eurjchem-1369	155	2	°	°	PROPN
eurjchem-1369	155	3	c	c	X
eurjchem-1369	155	4	.	.	PUNCT
eurjchem-1369	156	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	156	2	(	(	PUNCT
eurjchem-1369	156	3	kbr	kbr	PROPN
eurjchem-1369	156	4	,	,	PUNCT
eurjchem-1369	156	5			PROPN
eurjchem-1369	156	6	,	,	PUNCT
eurjchem-1369	156	7	cm‐1	cm‐1	PROPN
eurjchem-1369	156	8	):	):	PUNCT
eurjchem-1369	156	9	3438‐3349	3438‐3349	NUM
eurjchem-1369	156	10	(	(	PUNCT
eurjchem-1369	156	11	nh2	nh2	PROPN
eurjchem-1369	156	12	)	)	PUNCT
eurjchem-1369	156	13	,	,	PUNCT
eurjchem-1369	156	14	3214	3214	NUM
eurjchem-1369	156	15	(	(	PUNCT
eurjchem-1369	156	16	nh	nh	NOUN
eurjchem-1369	156	17	)	)	PUNCT
eurjchem-1369	156	18	,	,	PUNCT
eurjchem-1369	156	19	2235	2235	NUM
eurjchem-1369	156	20	(	(	PUNCT
eurjchem-1369	156	21	cn	cn	NOUN
eurjchem-1369	156	22	)	)	PUNCT
eurjchem-1369	156	23	,	,	PUNCT
eurjchem-1369	156	24	1686	1686	NUM
eurjchem-1369	156	25	,	,	PUNCT
eurjchem-1369	156	26	1652	1652	NUM
eurjchem-1369	156	27	,	,	PUNCT
eurjchem-1369	156	28	1633	1633	NUM
eurjchem-1369	156	29	(	(	PUNCT
eurjchem-1369	156	30	c	c	X
eurjchem-1369	156	31	=	=	SYM
eurjchem-1369	156	32	o	o	NOUN
eurjchem-1369	156	33	's	's	PART
eurjchem-1369	156	34	)	)	PUNCT
eurjchem-1369	156	35	.	.	PUNCT
eurjchem-1369	157	1	1h	1h	NUM
eurjchem-1369	157	2	nmr	nmr	NOUN
eurjchem-1369	157	3	(	(	PUNCT
eurjchem-1369	157	4	250	250	NUM
eurjchem-1369	157	5	mhz	mhz	NOUN
eurjchem-1369	157	6	,	,	PUNCT
eurjchem-1369	157	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	157	8	,	,	PUNCT
eurjchem-1369	157	9	δ	δ	PROPN
eurjchem-1369	157	10	,	,	PUNCT
eurjchem-1369	157	11	ppm	ppm	NUM
eurjchem-1369	157	12	):	):	PUNCT
eurjchem-1369	157	13	1.15‐1.23	1.15‐1.23	NUM
eurjchem-1369	157	14	(	(	PUNCT
eurjchem-1369	157	15	t	t	PROPN
eurjchem-1369	157	16	,	,	PUNCT
eurjchem-1369	157	17	3h	3h	NUM
eurjchem-1369	157	18	,	,	PUNCT
eurjchem-1369	157	19	ch3	ch3	PROPN
eurjchem-1369	157	20	)	)	PUNCT
eurjchem-1369	157	21	,	,	PUNCT
eurjchem-1369	157	22	3.77	3.77	NUM
eurjchem-1369	157	23	(	(	PUNCT
eurjchem-1369	157	24	s	s	PROPN
eurjchem-1369	157	25	,	,	PUNCT
eurjchem-1369	157	26	1h	1h	NUM
eurjchem-1369	157	27	,	,	PUNCT
eurjchem-1369	157	28	pyrimidine‐nh	pyrimidine‐nh	PROPN
eurjchem-1369	157	29	)	)	PUNCT
eurjchem-1369	157	30	,	,	PUNCT
eurjchem-1369	157	31	4.25	4.25	NUM
eurjchem-1369	157	32	(	(	PUNCT
eurjchem-1369	157	33	s	s	PROPN
eurjchem-1369	157	34	,	,	PUNCT
eurjchem-1369	157	35	2h	2h	NUM
eurjchem-1369	157	36	,	,	PUNCT
eurjchem-1369	157	37	ch2	ch2	PROPN
eurjchem-1369	157	38	)	)	PUNCT
eurjchem-1369	157	39	,	,	PUNCT
eurjchem-1369	157	40	4.45‐4.38	4.45‐4.38	NUM
eurjchem-1369	157	41	(	(	PUNCT
eurjchem-1369	157	42	q	q	NOUN
eurjchem-1369	157	43	,	,	PUNCT
eurjchem-1369	157	44	2h	2h	NUM
eurjchem-1369	157	45	,	,	PUNCT
eurjchem-1369	157	46	ch2	ch2	PROPN
eurjchem-1369	157	47	)	)	PUNCT
eurjchem-1369	157	48	,	,	PUNCT
eurjchem-1369	157	49	6.65	6.65	NUM
eurjchem-1369	157	50	(	(	PUNCT
eurjchem-1369	157	51	s	s	NOUN
eurjchem-1369	157	52	,	,	PUNCT
eurjchem-1369	157	53	2h	2h	NUM
eurjchem-1369	157	54	,	,	PUNCT
eurjchem-1369	157	55	nh2	nh2	PROPN
eurjchem-1369	157	56	)	)	PUNCT
eurjchem-1369	157	57	7.35‐7.75	7.35‐7.75	PROPN
eurjchem-1369	157	58	(	(	PUNCT
eurjchem-1369	157	59	m	m	PROPN
eurjchem-1369	157	60	,	,	PUNCT
eurjchem-1369	157	61	5h	5h	NUM
eurjchem-1369	157	62	,	,	PUNCT
eurjchem-1369	157	63	ar‐h	ar‐h	NOUN
eurjchem-1369	157	64	)	)	PUNCT
eurjchem-1369	157	65	,	,	PUNCT
eurjchem-1369	157	66	8.78	8.78	NUM
eurjchem-1369	157	67	(	(	PUNCT
eurjchem-1369	157	68	s	s	PROPN
eurjchem-1369	157	69	,	,	PUNCT
eurjchem-1369	157	70	1h	1h	NUM
eurjchem-1369	157	71	,	,	PUNCT
eurjchem-1369	157	72	nh	nh	PROPN
eurjchem-1369	157	73	)	)	PUNCT
eurjchem-1369	157	74	.	.	PUNCT
eurjchem-1369	158	1	ms	ms	NOUN
eurjchem-1369	158	2	(	(	PUNCT
eurjchem-1369	158	3	ei	ei	PROPN
eurjchem-1369	158	4	,	,	PUNCT
eurjchem-1369	158	5	m	m	PROPN
eurjchem-1369	158	6	/	/	SYM
eurjchem-1369	158	7	z	z	PROPN
eurjchem-1369	158	8	(	(	PUNCT
eurjchem-1369	158	9	%	%	NOUN
eurjchem-1369	158	10	)	)	PUNCT
eurjchem-1369	158	11	):	):	PUNCT
eurjchem-1369	158	12	412	412	NUM
eurjchem-1369	158	13	(	(	PUNCT
eurjchem-1369	158	14	m+	m+	NUM
eurjchem-1369	158	15	,	,	PUNCT
eurjchem-1369	158	16	26	26	NUM
eurjchem-1369	158	17	)	)	PUNCT
eurjchem-1369	158	18	.	.	PUNCT
eurjchem-1369	159	1	anal	anal	PROPN
eurjchem-1369	159	2	.	.	PUNCT
eurjchem-1369	159	3	calcd	calcd	NOUN
eurjchem-1369	159	4	.	.	PUNCT
eurjchem-1369	160	1	for	for	ADP
eurjchem-1369	160	2	c18h16n6o4s	c18h16n6o4s	NUM
eurjchem-1369	160	3	:	:	PUNCT
eurjchem-1369	160	4	c	c	NOUN
eurjchem-1369	160	5	,	,	PUNCT
eurjchem-1369	160	6	52.42	52.42	NUM
eurjchem-1369	160	7	;	;	PUNCT
eurjchem-1369	160	8	h	h	X
eurjchem-1369	160	9	,	,	PUNCT
eurjchem-1369	160	10	3.91	3.91	NUM
eurjchem-1369	160	11	;	;	PUNCT
eurjchem-1369	160	12	n	n	CCONJ
eurjchem-1369	160	13	,	,	PUNCT
eurjchem-1369	160	14	20.38	20.38	NUM
eurjchem-1369	160	15	.	.	PUNCT
eurjchem-1369	160	16	found	find	VERB
eurjchem-1369	160	17	:	:	PUNCT
eurjchem-1369	161	1	c	c	X
eurjchem-1369	161	2	,	,	PUNCT
eurjchem-1369	161	3	52.45	52.45	NUM
eurjchem-1369	161	4	;	;	PUNCT
eurjchem-1369	161	5	h	h	NOUN
eurjchem-1369	161	6	,	,	PUNCT
eurjchem-1369	161	7	4.10	4.10	NUM
eurjchem-1369	161	8	;	;	PUNCT
eurjchem-1369	161	9	n	n	CCONJ
eurjchem-1369	161	10	,	,	PUNCT
eurjchem-1369	161	11	20.46	20.46	NUM
eurjchem-1369	161	12	%	%	NOUN
eurjchem-1369	161	13	.	.	PUNCT
eurjchem-1369	162	1	6‐cyano‐7‐oxo‐5‐phenylamino‐2‐ureido‐4	6‐cyano‐7‐oxo‐5‐phenylamino‐2‐ureido‐4	NOUN
eurjchem-1369	162	2	,	,	PUNCT
eurjchem-1369	162	3	7‐dihydro‐pyra	7‐dihydro‐pyra	PROPN
eurjchem-1369	162	4	zolo[1,5‐a]pyrimidine‐3‐carboxylic	zolo[1,5‐a]pyrimidine‐3‐carboxylic	PROPN
eurjchem-1369	162	5	acid	acid	PROPN
eurjchem-1369	162	6	ethyl	ethyl	PROPN
eurjchem-1369	162	7	ester	ester	NOUN
eurjchem-1369	162	8	(	(	PUNCT
eurjchem-1369	162	9	10b	10b	NOUN
eurjchem-1369	162	10	):	):	PUNCT
eurjchem-1369	162	11	color	color	NOUN
eurjchem-1369	162	12	:	:	PUNCT
eurjchem-1369	162	13	yellow	yellow	ADJ
eurjchem-1369	162	14	crystals	crystal	NOUN
eurjchem-1369	162	15	.	.	PUNCT
eurjchem-1369	163	1	yield	yield	NOUN
eurjchem-1369	163	2	:	:	PUNCT
eurjchem-1369	163	3	51	51	NUM
eurjchem-1369	163	4	%	%	NOUN
eurjchem-1369	163	5	.	.	PUNCT
eurjchem-1369	164	1	m.p	m.p	PROPN
eurjchem-1369	164	2	.	.	PROPN
eurjchem-1369	164	3	:	:	PUNCT
eurjchem-1369	165	1	343‐345	343‐345	NUM
eurjchem-1369	165	2	°	°	ADP
eurjchem-1369	165	3	c	c	X
eurjchem-1369	165	4	.	.	PUNCT
eurjchem-1369	166	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	166	2	(	(	PUNCT
eurjchem-1369	166	3	kbr	kbr	PROPN
eurjchem-1369	166	4	,	,	PUNCT
eurjchem-1369	166	5			PROPN
eurjchem-1369	166	6	,	,	PUNCT
eurjchem-1369	166	7	cm‐1	cm‐1	PROPN
eurjchem-1369	166	8	):	):	PUNCT
eurjchem-1369	166	9	3465‐3340	3465‐3340	PROPN
eurjchem-1369	166	10	(	(	PUNCT
eurjchem-1369	166	11	nh2	nh2	PROPN
eurjchem-1369	166	12	)	)	PUNCT
eurjchem-1369	166	13	,	,	PUNCT
eurjchem-1369	166	14	3114‐3285	3114‐3285	NUM
eurjchem-1369	166	15	(	(	PUNCT
eurjchem-1369	166	16	nh	nh	NOUN
eurjchem-1369	166	17	)	)	PUNCT
eurjchem-1369	166	18	,	,	PUNCT
eurjchem-1369	166	19	2205	2205	NUM
eurjchem-1369	166	20	(	(	PUNCT
eurjchem-1369	166	21	cn	cn	PROPN
eurjchem-1369	166	22	)	)	PUNCT
eurjchem-1369	166	23	,	,	PUNCT
eurjchem-1369	166	24	1725	1725	NUM
eurjchem-1369	166	25	,	,	PUNCT
eurjchem-1369	166	26	1655	1655	NUM
eurjchem-1369	166	27	(	(	PUNCT
eurjchem-1369	166	28	c	c	X
eurjchem-1369	166	29	=	=	SYM
eurjchem-1369	166	30	o	o	NOUN
eurjchem-1369	166	31	's	's	PART
eurjchem-1369	166	32	)	)	PUNCT
eurjchem-1369	166	33	.	.	PUNCT
eurjchem-1369	167	1	1h	1h	NUM
eurjchem-1369	167	2	nmr	nmr	NOUN
eurjchem-1369	167	3	(	(	PUNCT
eurjchem-1369	167	4	250	250	NUM
eurjchem-1369	167	5	mhz	mhz	NOUN
eurjchem-1369	167	6	,	,	PUNCT
eurjchem-1369	167	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	167	8	,	,	PUNCT
eurjchem-1369	167	9	δ	δ	PROPN
eurjchem-1369	167	10	,	,	PUNCT
eurjchem-1369	167	11	ppm	ppm	NUM
eurjchem-1369	167	12	):	):	PUNCT
eurjchem-1369	167	13	1.32‐1.22	1.32‐1.22	NUM
eurjchem-1369	167	14	(	(	PUNCT
eurjchem-1369	167	15	t	t	PROPN
eurjchem-1369	167	16	,	,	PUNCT
eurjchem-1369	167	17	3h	3h	NUM
eurjchem-1369	167	18	,	,	PUNCT
eurjchem-1369	167	19	ch3	ch3	PROPN
eurjchem-1369	167	20	)	)	PUNCT
eurjchem-1369	167	21	,	,	PUNCT
eurjchem-1369	167	22	3.8	3.8	NUM
eurjchem-1369	167	23	(	(	PUNCT
eurjchem-1369	167	24	s	s	PROPN
eurjchem-1369	167	25	,	,	PUNCT
eurjchem-1369	167	26	1h	1h	NUM
eurjchem-1369	167	27	,	,	PUNCT
eurjchem-1369	167	28	pyrimidine‐nh	pyrimidine‐nh	PROPN
eurjchem-1369	167	29	)	)	PUNCT
eurjchem-1369	167	30	,	,	PUNCT
eurjchem-1369	167	31	4.66	4.66	NUM
eurjchem-1369	167	32	(	(	PUNCT
eurjchem-1369	167	33	s	s	PROPN
eurjchem-1369	167	34	,	,	PUNCT
eurjchem-1369	167	35	1h	1h	NUM
eurjchem-1369	167	36	,	,	PUNCT
eurjchem-1369	167	37	nh‐ph	nh‐ph	NUM
eurjchem-1369	167	38	)	)	PUNCT
eurjchem-1369	167	39	,	,	PUNCT
eurjchem-1369	167	40	4.42‐4.15	4.42‐4.15	NUM
eurjchem-1369	167	41	(	(	PUNCT
eurjchem-1369	167	42	q	q	NOUN
eurjchem-1369	167	43	,	,	PUNCT
eurjchem-1369	167	44	2h	2h	NUM
eurjchem-1369	167	45	,	,	PUNCT
eurjchem-1369	167	46	ch2	ch2	PROPN
eurjchem-1369	167	47	)	)	PUNCT
eurjchem-1369	167	48	,	,	PUNCT
eurjchem-1369	167	49	5.63	5.63	NUM
eurjchem-1369	167	50	(	(	PUNCT
eurjchem-1369	167	51	s	s	PROPN
eurjchem-1369	167	52	,	,	PUNCT
eurjchem-1369	167	53	2h	2h	NUM
eurjchem-1369	167	54	,	,	PUNCT
eurjchem-1369	167	55	nh2	nh2	PROPN
eurjchem-1369	167	56	)	)	PUNCT
eurjchem-1369	167	57	,	,	PUNCT
eurjchem-1369	167	58	8.53	8.53	NUM
eurjchem-1369	167	59	(	(	PUNCT
eurjchem-1369	167	60	s	s	PROPN
eurjchem-1369	167	61	,	,	PUNCT
eurjchem-1369	167	62	1h	1h	NUM
eurjchem-1369	167	63	,	,	PUNCT
eurjchem-1369	167	64	nh	nh	PROPN
eurjchem-1369	167	65	)	)	PUNCT
eurjchem-1369	167	66	,	,	PUNCT
eurjchem-1369	167	67	7.05‐	7.05‐	NUM
eurjchem-1369	167	68	110	110	NUM
eurjchem-1369	167	69	abbas‐temirek	abbas‐temirek	NOUN
eurjchem-1369	167	70	and	and	CCONJ
eurjchem-1369	167	71	abo‐bakr	abo‐bakr	ADJ
eurjchem-1369	167	72	/	/	SYM
eurjchem-1369	167	73	european	european	ADJ
eurjchem-1369	167	74	journal	journal	PROPN
eurjchem-1369	167	75	of	of	ADP
eurjchem-1369	167	76	chemistry	chemistry	NOUN
eurjchem-1369	167	77	7	7	NUM
eurjchem-1369	167	78	(	(	PUNCT
eurjchem-1369	167	79	1	1	NUM
eurjchem-1369	167	80	)	)	PUNCT
eurjchem-1369	167	81	(	(	PUNCT
eurjchem-1369	167	82	2016	2016	NUM
eurjchem-1369	167	83	)	)	PUNCT
eurjchem-1369	167	84	107‐114	107‐114	NUM
eurjchem-1369	167	85	scheme	scheme	NOUN
eurjchem-1369	167	86	3	3	NUM
eurjchem-1369	167	87	7.45	7.45	NUM
eurjchem-1369	167	88	(	(	PUNCT
eurjchem-1369	167	89	m	m	PROPN
eurjchem-1369	167	90	,	,	PUNCT
eurjchem-1369	167	91	5h	5h	NUM
eurjchem-1369	167	92	,	,	PUNCT
eurjchem-1369	167	93	ar‐h	ar‐h	NOUN
eurjchem-1369	167	94	)	)	PUNCT
eurjchem-1369	167	95	.	.	PUNCT
eurjchem-1369	168	1	ms	ms	NOUN
eurjchem-1369	168	2	(	(	PUNCT
eurjchem-1369	168	3	ei	ei	PROPN
eurjchem-1369	168	4	,	,	PUNCT
eurjchem-1369	168	5	m	m	PROPN
eurjchem-1369	168	6	/	/	SYM
eurjchem-1369	168	7	z	z	PROPN
eurjchem-1369	168	8	(	(	PUNCT
eurjchem-1369	168	9	%	%	NOUN
eurjchem-1369	168	10	)	)	PUNCT
eurjchem-1369	168	11	):	):	PUNCT
eurjchem-1369	168	12	381	381	NUM
eurjchem-1369	168	13	(	(	PUNCT
eurjchem-1369	168	14	m+	m+	NUM
eurjchem-1369	168	15	,	,	PUNCT
eurjchem-1369	168	16	11	11	NUM
eurjchem-1369	168	17	)	)	PUNCT
eurjchem-1369	168	18	.	.	PUNCT
eurjchem-1369	169	1	anal	anal	PROPN
eurjchem-1369	169	2	.	.	PUNCT
eurjchem-1369	169	3	calcd	calcd	NOUN
eurjchem-1369	169	4	.	.	PUNCT
eurjchem-1369	170	1	for	for	ADP
eurjchem-1369	170	2	c17h15n7o4	c17h15n7o4	NOUN
eurjchem-1369	170	3	:	:	PUNCT
eurjchem-1369	170	4	c	c	X
eurjchem-1369	170	5	,	,	PUNCT
eurjchem-1369	170	6	53.54	53.54	NUM
eurjchem-1369	170	7	;	;	PUNCT
eurjchem-1369	170	8	h	h	NOUN
eurjchem-1369	170	9	,	,	PUNCT
eurjchem-1369	170	10	3.96	3.96	NUM
eurjchem-1369	170	11	;	;	PUNCT
eurjchem-1369	170	12	n	n	CCONJ
eurjchem-1369	170	13	,	,	PUNCT
eurjchem-1369	170	14	25.71	25.71	NUM
eurjchem-1369	170	15	.	.	PUNCT
eurjchem-1369	170	16	found	find	VERB
eurjchem-1369	170	17	:	:	PUNCT
eurjchem-1369	171	1	c	c	X
eurjchem-1369	171	2	,	,	PUNCT
eurjchem-1369	171	3	53.65	53.65	NUM
eurjchem-1369	171	4	;	;	PUNCT
eurjchem-1369	172	1	h	h	NOUN
eurjchem-1369	172	2	,	,	PUNCT
eurjchem-1369	172	3	4.15	4.15	NUM
eurjchem-1369	172	4	;	;	PUNCT
eurjchem-1369	172	5	n	n	CCONJ
eurjchem-1369	172	6	,	,	PUNCT
eurjchem-1369	172	7	25.55	25.55	NUM
eurjchem-1369	172	8	%	%	NOUN
eurjchem-1369	172	9	.	.	PUNCT
eurjchem-1369	173	1	6‐cyano‐7‐oxo‐2,5‐diureido‐4,7‐dihydro‐pyrazolo[1,5‐a]pyri	6‐cyano‐7‐oxo‐2,5‐diureido‐4,7‐dihydro‐pyrazolo[1,5‐a]pyri	NUM
eurjchem-1369	173	2	midine‐3‐carboxylic	midine‐3‐carboxylic	NUM
eurjchem-1369	173	3	acid	acid	PROPN
eurjchem-1369	173	4	ethyl	ethyl	PROPN
eurjchem-1369	173	5	ester	ester	NOUN
eurjchem-1369	173	6	(	(	PUNCT
eurjchem-1369	173	7	10c	10c	NUM
eurjchem-1369	173	8	):	):	PUNCT
eurjchem-1369	173	9	color	color	NOUN
eurjchem-1369	173	10	:	:	PUNCT
eurjchem-1369	173	11	colourless	colourless	ADJ
eurjchem-1369	173	12	crystals	crystal	NOUN
eurjchem-1369	173	13	.	.	PUNCT
eurjchem-1369	174	1	yield	yield	NOUN
eurjchem-1369	174	2	:	:	PUNCT
eurjchem-1369	174	3	60	60	NUM
eurjchem-1369	174	4	%	%	NOUN
eurjchem-1369	174	5	.	.	PUNCT
eurjchem-1369	175	1	m.p	m.p	PROPN
eurjchem-1369	175	2	.	.	PROPN
eurjchem-1369	175	3	:	:	PUNCT
eurjchem-1369	176	1	341‐343	341‐343	PROPN
eurjchem-1369	176	2	°	°	SYM
eurjchem-1369	176	3	c	c	PROPN
eurjchem-1369	176	4	.	.	PUNCT
eurjchem-1369	177	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	177	2	(	(	PUNCT
eurjchem-1369	177	3	kbr	kbr	PROPN
eurjchem-1369	177	4	,	,	PUNCT
eurjchem-1369	177	5			PROPN
eurjchem-1369	177	6	,	,	PUNCT
eurjchem-1369	177	7	cm‐1	cm‐1	PROPN
eurjchem-1369	177	8	):	):	PUNCT
eurjchem-1369	177	9	3413‐3211	3413‐3211	NUM
eurjchem-1369	177	10	(	(	PUNCT
eurjchem-1369	177	11	nh2	nh2	PROPN
eurjchem-1369	177	12	and	and	CCONJ
eurjchem-1369	177	13	nh	nh	PROPN
eurjchem-1369	177	14	)	)	PUNCT
eurjchem-1369	177	15	,	,	PUNCT
eurjchem-1369	177	16	2221	2221	NUM
eurjchem-1369	177	17	(	(	PUNCT
eurjchem-1369	177	18	cn	cn	PROPN
eurjchem-1369	177	19	)	)	PUNCT
eurjchem-1369	177	20	,	,	PUNCT
eurjchem-1369	177	21	1684	1684	NUM
eurjchem-1369	177	22	,	,	PUNCT
eurjchem-1369	177	23	1652	1652	NUM
eurjchem-1369	177	24	(	(	PUNCT
eurjchem-1369	177	25	c	c	X
eurjchem-1369	177	26	=	=	SYM
eurjchem-1369	177	27	o	o	NOUN
eurjchem-1369	177	28	's	's	PART
eurjchem-1369	177	29	)	)	PUNCT
eurjchem-1369	177	30	.	.	PUNCT
eurjchem-1369	178	1	1h	1h	NUM
eurjchem-1369	178	2	nmr	nmr	NOUN
eurjchem-1369	178	3	(	(	PUNCT
eurjchem-1369	178	4	250	250	NUM
eurjchem-1369	178	5	mhz	mhz	NOUN
eurjchem-1369	178	6	,	,	PUNCT
eurjchem-1369	178	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	178	8	,	,	PUNCT
eurjchem-1369	178	9	δ	δ	PROPN
eurjchem-1369	178	10	,	,	PUNCT
eurjchem-1369	178	11	ppm	ppm	NUM
eurjchem-1369	178	12	):	):	PUNCT
eurjchem-1369	178	13	1.25‐1.15	1.25‐1.15	NUM
eurjchem-1369	178	14	(	(	PUNCT
eurjchem-1369	178	15	t	t	PROPN
eurjchem-1369	178	16	,	,	PUNCT
eurjchem-1369	178	17	3h	3h	NUM
eurjchem-1369	178	18	,	,	PUNCT
eurjchem-1369	178	19	ch3	ch3	PROPN
eurjchem-1369	178	20	)	)	PUNCT
eurjchem-1369	178	21	,	,	PUNCT
eurjchem-1369	178	22	3.90	3.90	NUM
eurjchem-1369	178	23	(	(	PUNCT
eurjchem-1369	178	24	s	s	PROPN
eurjchem-1369	178	25	,	,	PUNCT
eurjchem-1369	178	26	1h	1h	NUM
eurjchem-1369	178	27	,	,	PUNCT
eurjchem-1369	178	28	pyrimidine‐nh	pyrimidine‐nh	PROPN
eurjchem-1369	178	29	)	)	PUNCT
eurjchem-1369	178	30	,	,	PUNCT
eurjchem-1369	178	31	4.35‐4.18	4.35‐4.18	X
eurjchem-1369	178	32	(	(	PUNCT
eurjchem-1369	178	33	q	q	NOUN
eurjchem-1369	178	34	,	,	PUNCT
eurjchem-1369	178	35	2h	2h	NUM
eurjchem-1369	178	36	,	,	PUNCT
eurjchem-1369	178	37	ch2	ch2	PROPN
eurjchem-1369	178	38	)	)	PUNCT
eurjchem-1369	178	39	,	,	PUNCT
eurjchem-1369	178	40	5.8	5.8	NUM
eurjchem-1369	178	41	(	(	PUNCT
eurjchem-1369	178	42	s	s	PROPN
eurjchem-1369	178	43	,	,	PUNCT
eurjchem-1369	178	44	2h	2h	NUM
eurjchem-1369	178	45	,	,	PUNCT
eurjchem-1369	178	46	nh2	nh2	PROPN
eurjchem-1369	178	47	)	)	PUNCT
eurjchem-1369	178	48	,	,	PUNCT
eurjchem-1369	178	49	6.55‐6.65	6.55‐6.65	NUM
eurjchem-1369	178	50	(	(	PUNCT
eurjchem-1369	178	51	br.s	br.s	PROPN
eurjchem-1369	178	52	,	,	PUNCT
eurjchem-1369	178	53	2h	2h	NUM
eurjchem-1369	178	54	,	,	PUNCT
eurjchem-1369	178	55	nh2	nh2	PROPN
eurjchem-1369	178	56	)	)	PUNCT
eurjchem-1369	178	57	,	,	PUNCT
eurjchem-1369	178	58	8.49	8.49	NUM
eurjchem-1369	178	59	(	(	PUNCT
eurjchem-1369	178	60	s	s	PROPN
eurjchem-1369	178	61	,	,	PUNCT
eurjchem-1369	178	62	1h	1h	NUM
eurjchem-1369	178	63	,	,	PUNCT
eurjchem-1369	178	64	nh	nh	PROPN
eurjchem-1369	178	65	)	)	PUNCT
eurjchem-1369	178	66	,	,	PUNCT
eurjchem-1369	178	67	8.85	8.85	NUM
eurjchem-1369	178	68	(	(	PUNCT
eurjchem-1369	178	69	s	s	PROPN
eurjchem-1369	178	70	,	,	PUNCT
eurjchem-1369	178	71	1h	1h	NUM
eurjchem-1369	178	72	,	,	PUNCT
eurjchem-1369	178	73	nh	nh	PROPN
eurjchem-1369	178	74	)	)	PUNCT
eurjchem-1369	178	75	.	.	PUNCT
eurjchem-1369	179	1	ms	ms	NOUN
eurjchem-1369	179	2	(	(	PUNCT
eurjchem-1369	179	3	ei	ei	PROPN
eurjchem-1369	179	4	,	,	PUNCT
eurjchem-1369	179	5	m	m	PROPN
eurjchem-1369	179	6	/	/	SYM
eurjchem-1369	179	7	z	z	PROPN
eurjchem-1369	179	8	(	(	PUNCT
eurjchem-1369	179	9	%	%	NOUN
eurjchem-1369	179	10	)	)	PUNCT
eurjchem-1369	179	11	):	):	PUNCT
eurjchem-1369	179	12	348	348	NUM
eurjchem-1369	179	13	(	(	PUNCT
eurjchem-1369	179	14	m+	m+	NUM
eurjchem-1369	179	15	,	,	PUNCT
eurjchem-1369	179	16	10	10	NUM
eurjchem-1369	179	17	)	)	PUNCT
eurjchem-1369	179	18	.	.	PUNCT
eurjchem-1369	180	1	anal	anal	PROPN
eurjchem-1369	180	2	.	.	PUNCT
eurjchem-1369	180	3	calcd	calcd	NOUN
eurjchem-1369	180	4	.	.	PUNCT
eurjchem-1369	181	1	for	for	ADP
eurjchem-1369	181	2	c12h12n8o5	c12h12n8o5	PROPN
eurjchem-1369	181	3	:	:	PUNCT
eurjchem-1369	181	4	c	c	NOUN
eurjchem-1369	181	5	,	,	PUNCT
eurjchem-1369	181	6	41.38	41.38	NUM
eurjchem-1369	181	7	;	;	PUNCT
eurjchem-1369	181	8	h	h	NOUN
eurjchem-1369	181	9	,	,	PUNCT
eurjchem-1369	181	10	3.47	3.47	NUM
eurjchem-1369	181	11	;	;	PUNCT
eurjchem-1369	181	12	n	n	CCONJ
eurjchem-1369	181	13	,	,	PUNCT
eurjchem-1369	181	14	32.17	32.17	NUM
eurjchem-1369	181	15	.	.	PUNCT
eurjchem-1369	181	16	found	find	VERB
eurjchem-1369	181	17	:	:	PUNCT
eurjchem-1369	182	1	c	c	X
eurjchem-1369	182	2	,	,	PUNCT
eurjchem-1369	182	3	41.65	41.65	NUM
eurjchem-1369	182	4	;	;	PUNCT
eurjchem-1369	182	5	h	h	NOUN
eurjchem-1369	182	6	,	,	PUNCT
eurjchem-1369	182	7	3.78	3.78	NUM
eurjchem-1369	182	8	;	;	PUNCT
eurjchem-1369	182	9	n	n	CCONJ
eurjchem-1369	182	10	,	,	PUNCT
eurjchem-1369	182	11	32.45	32.45	NUM
eurjchem-1369	182	12	%	%	NOUN
eurjchem-1369	182	13	.	.	PUNCT
eurjchem-1369	183	1	6‐cyano‐5‐methylsulfanyl‐7‐oxo‐2‐ureido‐4	6‐cyano‐5‐methylsulfanyl‐7‐oxo‐2‐ureido‐4	NUM
eurjchem-1369	183	2	,	,	PUNCT
eurjchem-1369	183	3	7‐dihydro‐pyra	7‐dihydro‐pyra	PROPN
eurjchem-1369	183	4	zolo[1,5‐a]pyrimidine‐3‐carboxylic	zolo[1,5‐a]pyrimidine‐3‐carboxylic	PROPN
eurjchem-1369	183	5	acid	acid	PROPN
eurjchem-1369	183	6	ethyl	ethyl	PROPN
eurjchem-1369	183	7	ester	ester	NOUN
eurjchem-1369	183	8	(	(	PUNCT
eurjchem-1369	183	9	11	11	NUM
eurjchem-1369	183	10	):	):	PUNCT
eurjchem-1369	183	11	color	color	NOUN
eurjchem-1369	183	12	:	:	PUNCT
eurjchem-1369	183	13	colourless	colourless	ADJ
eurjchem-1369	183	14	crystals	crystal	NOUN
eurjchem-1369	183	15	.	.	PUNCT
eurjchem-1369	184	1	yield	yield	NOUN
eurjchem-1369	184	2	:	:	PUNCT
eurjchem-1369	184	3	69	69	NUM
eurjchem-1369	184	4	%	%	NOUN
eurjchem-1369	184	5	.	.	PUNCT
eurjchem-1369	185	1	m.p	m.p	PROPN
eurjchem-1369	185	2	.	.	PROPN
eurjchem-1369	185	3	:	:	PUNCT
eurjchem-1369	186	1	358‐360	358‐360	NUM
eurjchem-1369	186	2	°	°	NOUN
eurjchem-1369	186	3	c	c	NOUN
eurjchem-1369	186	4	.	.	PUNCT
eurjchem-1369	187	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	187	2	(	(	PUNCT
eurjchem-1369	187	3	kbr	kbr	PROPN
eurjchem-1369	187	4	,	,	PUNCT
eurjchem-1369	187	5			PROPN
eurjchem-1369	187	6	,	,	PUNCT
eurjchem-1369	187	7	cm‐1	cm‐1	PROPN
eurjchem-1369	187	8	):	):	PUNCT
eurjchem-1369	187	9	3374‐3495	3374‐3495	NUM
eurjchem-1369	187	10	(	(	PUNCT
eurjchem-1369	187	11	2nh2	2nh2	NUM
eurjchem-1369	187	12	)	)	PUNCT
eurjchem-1369	187	13	,	,	PUNCT
eurjchem-1369	187	14	3158	3158	NUM
eurjchem-1369	187	15	(	(	PUNCT
eurjchem-1369	187	16	nh	nh	NOUN
eurjchem-1369	187	17	)	)	PUNCT
eurjchem-1369	187	18	,	,	PUNCT
eurjchem-1369	187	19	2230	2230	NUM
eurjchem-1369	187	20	(	(	PUNCT
eurjchem-1369	187	21	cn	cn	PROPN
eurjchem-1369	187	22	)	)	PUNCT
eurjchem-1369	187	23	,	,	PUNCT
eurjchem-1369	187	24	1705	1705	NUM
eurjchem-1369	187	25	,	,	PUNCT
eurjchem-1369	187	26	1662	1662	NUM
eurjchem-1369	187	27	(	(	PUNCT
eurjchem-1369	187	28	c	c	X
eurjchem-1369	187	29	=	=	SYM
eurjchem-1369	187	30	o	o	NOUN
eurjchem-1369	187	31	's	's	PART
eurjchem-1369	187	32	)	)	PUNCT
eurjchem-1369	187	33	.	.	PUNCT
eurjchem-1369	188	1	1h	1h	NUM
eurjchem-1369	188	2	nmr	nmr	NOUN
eurjchem-1369	188	3	(	(	PUNCT
eurjchem-1369	188	4	250	250	NUM
eurjchem-1369	188	5	mhz	mhz	NOUN
eurjchem-1369	188	6	,	,	PUNCT
eurjchem-1369	188	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	188	8	,	,	PUNCT
eurjchem-1369	188	9	δ	δ	PROPN
eurjchem-1369	188	10	,	,	PUNCT
eurjchem-1369	188	11	ppm	ppm	NUM
eurjchem-1369	188	12	):	):	PUNCT
eurjchem-1369	188	13	2.50‐2.47	2.50‐2.47	NUM
eurjchem-1369	188	14	(	(	PUNCT
eurjchem-1369	188	15	t	t	PROPN
eurjchem-1369	188	16	,	,	PUNCT
eurjchem-1369	188	17	3h	3h	NUM
eurjchem-1369	188	18	,	,	PUNCT
eurjchem-1369	188	19	ch3	ch3	PROPN
eurjchem-1369	188	20	)	)	PUNCT
eurjchem-1369	188	21	,	,	PUNCT
eurjchem-1369	188	22	2.45	2.45	NUM
eurjchem-1369	188	23	(	(	PUNCT
eurjchem-1369	188	24	s	s	PROPN
eurjchem-1369	188	25	,	,	PUNCT
eurjchem-1369	188	26	3h	3h	NUM
eurjchem-1369	188	27	,	,	PUNCT
eurjchem-1369	188	28	sme	sme	NOUN
eurjchem-1369	188	29	)	)	PUNCT
eurjchem-1369	188	30	,	,	PUNCT
eurjchem-1369	188	31	3.88	3.88	NUM
eurjchem-1369	188	32	(	(	PUNCT
eurjchem-1369	188	33	s	s	PROPN
eurjchem-1369	188	34	,	,	PUNCT
eurjchem-1369	188	35	1h	1h	NUM
eurjchem-1369	188	36	,	,	PUNCT
eurjchem-1369	188	37	pyrimidine‐nh	pyrimidine‐nh	PROPN
eurjchem-1369	188	38	)	)	PUNCT
eurjchem-1369	188	39	,	,	PUNCT
eurjchem-1369	188	40	4.26‐4.35	4.26‐4.35	NUM
eurjchem-1369	188	41	(	(	PUNCT
eurjchem-1369	188	42	q	q	NOUN
eurjchem-1369	188	43	,	,	PUNCT
eurjchem-1369	188	44	2h	2h	NUM
eurjchem-1369	188	45	,	,	PUNCT
eurjchem-1369	188	46	‐ch2	‐ch2	NUM
eurjchem-1369	188	47	)	)	PUNCT
eurjchem-1369	188	48	,	,	PUNCT
eurjchem-1369	188	49	7.17	7.17	NUM
eurjchem-1369	188	50	(	(	PUNCT
eurjchem-1369	188	51	br.s	br.s	PROPN
eurjchem-1369	188	52	,	,	PUNCT
eurjchem-1369	188	53	2h	2h	NUM
eurjchem-1369	188	54	,	,	PUNCT
eurjchem-1369	188	55	nh2	nh2	PROPN
eurjchem-1369	188	56	)	)	PUNCT
eurjchem-1369	188	57	,	,	PUNCT
eurjchem-1369	188	58	8.32	8.32	NUM
eurjchem-1369	188	59	(	(	PUNCT
eurjchem-1369	188	60	s	s	PROPN
eurjchem-1369	188	61	,	,	PUNCT
eurjchem-1369	188	62	1h	1h	NUM
eurjchem-1369	188	63	,	,	PUNCT
eurjchem-1369	188	64	nh	nh	PROPN
eurjchem-1369	188	65	)	)	PUNCT
eurjchem-1369	188	66	.	.	PUNCT
eurjchem-1369	189	1	ms	ms	NOUN
eurjchem-1369	189	2	(	(	PUNCT
eurjchem-1369	189	3	ei	ei	PROPN
eurjchem-1369	189	4	,	,	PUNCT
eurjchem-1369	189	5	m	m	PROPN
eurjchem-1369	189	6	/	/	SYM
eurjchem-1369	189	7	z	z	PROPN
eurjchem-1369	189	8	(	(	PUNCT
eurjchem-1369	189	9	%	%	NOUN
eurjchem-1369	189	10	)	)	PUNCT
eurjchem-1369	189	11	):	):	PUNCT
eurjchem-1369	189	12	336	336	NUM
eurjchem-1369	189	13	(	(	PUNCT
eurjchem-1369	189	14	m+	m+	NUM
eurjchem-1369	189	15	,	,	PUNCT
eurjchem-1369	189	16	13	13	NUM
eurjchem-1369	189	17	)	)	PUNCT
eurjchem-1369	189	18	.	.	PUNCT
eurjchem-1369	190	1	anal	anal	PROPN
eurjchem-1369	190	2	.	.	PUNCT
eurjchem-1369	190	3	calcd	calcd	NOUN
eurjchem-1369	190	4	.	.	PUNCT
eurjchem-1369	191	1	for	for	SCONJ
eurjchem-1369	191	2	c12h12n6o4s	c12h12n6o4s	NUM
eurjchem-1369	191	3	:	:	PUNCT
eurjchem-1369	191	4	c	c	X
eurjchem-1369	191	5	,	,	PUNCT
eurjchem-1369	191	6	42.85	42.85	NUM
eurjchem-1369	191	7	;	;	PUNCT
eurjchem-1369	191	8	h	h	NOUN
eurjchem-1369	191	9	,	,	PUNCT
eurjchem-1369	191	10	3.60	3.60	NUM
eurjchem-1369	191	11	;	;	PUNCT
eurjchem-1369	191	12	n	n	CCONJ
eurjchem-1369	191	13	,	,	PUNCT
eurjchem-1369	191	14	24.99	24.99	NUM
eurjchem-1369	191	15	.	.	PUNCT
eurjchem-1369	191	16	found	find	VERB
eurjchem-1369	191	17	:	:	PUNCT
eurjchem-1369	192	1	c	c	X
eurjchem-1369	192	2	,	,	PUNCT
eurjchem-1369	192	3	42.56	42.56	NUM
eurjchem-1369	192	4	;	;	PUNCT
eurjchem-1369	192	5	h	h	NOUN
eurjchem-1369	192	6	,	,	PUNCT
eurjchem-1369	192	7	3.66	3.66	NUM
eurjchem-1369	192	8	;	;	PUNCT
eurjchem-1369	192	9	n	n	CCONJ
eurjchem-1369	192	10	,	,	PUNCT
eurjchem-1369	192	11	25.28	25.28	NUM
eurjchem-1369	192	12	%	%	NOUN
eurjchem-1369	192	13	.	.	PUNCT
eurjchem-1369	193	1	2.2.6	2.2.6	X
eurjchem-1369	193	2	.	.	PUNCT
eurjchem-1369	193	3	general	general	ADJ
eurjchem-1369	193	4	procedure	procedure	NOUN
eurjchem-1369	193	5	for	for	ADP
eurjchem-1369	193	6	the	the	DET
eurjchem-1369	193	7	reactions	reaction	NOUN
eurjchem-1369	193	8	of	of	ADP
eurjchem-1369	193	9	compound	compound	NOUN
eurjchem-1369	193	10	4a	4a	NOUN
eurjchem-1369	193	11	with	with	ADP
eurjchem-1369	193	12	ethoxymethylenemalononitrile	ethoxymethylenemalononitrile	ADJ
eurjchem-1369	193	13	and	and	CCONJ
eurjchem-1369	193	14	ethoxymethylene	ethoxymethylene	NOUN
eurjchem-1369	193	15	cyanoacetate	cyanoacetate	NOUN
eurjchem-1369	193	16	to	to	ADP
eurjchem-1369	193	17	a	a	DET
eurjchem-1369	193	18	solution	solution	NOUN
eurjchem-1369	193	19	of	of	ADP
eurjchem-1369	193	20	compound	compound	NOUN
eurjchem-1369	193	21	4a	4a	NOUN
eurjchem-1369	193	22	(	(	PUNCT
eurjchem-1369	193	23	2.13	2.13	NUM
eurjchem-1369	193	24	g	g	NOUN
eurjchem-1369	193	25	,	,	PUNCT
eurjchem-1369	193	26	0.01	0.01	NUM
eurjchem-1369	193	27	mole	mole	NOUN
eurjchem-1369	193	28	)	)	PUNCT
eurjchem-1369	193	29	in	in	ADP
eurjchem-1369	193	30	(	(	PUNCT
eurjchem-1369	193	31	10	10	NUM
eurjchem-1369	193	32	ml	ml	NOUN
eurjchem-1369	193	33	)	)	PUNCT
eurjchem-1369	193	34	acetic	acetic	ADJ
eurjchem-1369	193	35	acid	acid	NOUN
eurjchem-1369	193	36	,	,	PUNCT
eurjchem-1369	193	37	ethoxymethylene	ethoxymethylene	NOUN
eurjchem-1369	193	38	malononitrile	malononitrile	NOUN
eurjchem-1369	193	39	or	or	CCONJ
eurjchem-1369	193	40	ethoxy	ethoxy	ADJ
eurjchem-1369	193	41	methylene	methylene	NOUN
eurjchem-1369	193	42	cyanoacetate	cyanoacetate	NOUN
eurjchem-1369	193	43	(	(	PUNCT
eurjchem-1369	193	44	0.01	0.01	NUM
eurjchem-1369	193	45	mole	mole	NOUN
eurjchem-1369	193	46	)	)	PUNCT
eurjchem-1369	193	47	was	be	AUX
eurjchem-1369	193	48	added	add	VERB
eurjchem-1369	193	49	.	.	PUNCT
eurjchem-1369	194	1	the	the	DET
eurjchem-1369	194	2	reaction	reaction	NOUN
eurjchem-1369	194	3	mixture	mixture	NOUN
eurjchem-1369	194	4	was	be	AUX
eurjchem-1369	194	5	refluxed	refluxe	VERB
eurjchem-1369	194	6	for	for	ADP
eurjchem-1369	194	7	the	the	DET
eurjchem-1369	194	8	appropriate	appropriate	ADJ
eurjchem-1369	194	9	time	time	NOUN
eurjchem-1369	194	10	(	(	PUNCT
eurjchem-1369	194	11	4‐6	4‐6	PROPN
eurjchem-1369	194	12	h	h	NOUN
eurjchem-1369	194	13	)	)	PUNCT
eurjchem-1369	194	14	.	.	PUNCT
eurjchem-1369	195	1	after	after	ADP
eurjchem-1369	195	2	this	this	DET
eurjchem-1369	195	3	time	time	NOUN
eurjchem-1369	195	4	the	the	DET
eurjchem-1369	195	5	reaction	reaction	NOUN
eurjchem-1369	195	6	mixture	mixture	NOUN
eurjchem-1369	195	7	was	be	AUX
eurjchem-1369	195	8	poured	pour	VERB
eurjchem-1369	195	9	into	into	ADP
eurjchem-1369	195	10	water	water	NOUN
eurjchem-1369	195	11	.	.	PUNCT
eurjchem-1369	196	1	the	the	DET
eurjchem-1369	196	2	solid	solid	ADJ
eurjchem-1369	196	3	product	product	NOUN
eurjchem-1369	196	4	formed	form	VERB
eurjchem-1369	196	5	crystallized	crystallize	VERB
eurjchem-1369	196	6	from	from	ADP
eurjchem-1369	196	7	appropriate	appropriate	ADJ
eurjchem-1369	196	8	solvent	solvent	NOUN
eurjchem-1369	196	9	to	to	PART
eurjchem-1369	196	10	yield	yield	VERB
eurjchem-1369	196	11	compound	compound	NOUN
eurjchem-1369	196	12	13a	13a	NOUN
eurjchem-1369	196	13	and	and	CCONJ
eurjchem-1369	196	14	13b	13b	NOUN
eurjchem-1369	196	15	,	,	PUNCT
eurjchem-1369	196	16	respectively	respectively	ADV
eurjchem-1369	196	17	(	(	PUNCT
eurjchem-1369	196	18	scheme	scheme	NOUN
eurjchem-1369	196	19	4	4	NUM
eurjchem-1369	196	20	)	)	PUNCT
eurjchem-1369	196	21	.	.	PUNCT
eurjchem-1369	197	1	5‐amino‐6‐cyano‐2‐ureido‐pyrazolo[1	5‐amino‐6‐cyano‐2‐ureido‐pyrazolo[1	NUM
eurjchem-1369	197	2	,	,	PUNCT
eurjchem-1369	197	3	5‐a]pyrimidine‐3‐	5‐a]pyrimidine‐3‐	NUM
eurjchem-1369	197	4	carboxylic	carboxylic	ADJ
eurjchem-1369	197	5	acid	acid	NOUN
eurjchem-1369	197	6	ethyl	ethyl	PROPN
eurjchem-1369	197	7	ester	ester	NOUN
eurjchem-1369	197	8	(	(	PUNCT
eurjchem-1369	197	9	13a	13a	NOUN
eurjchem-1369	197	10	):	):	PUNCT
eurjchem-1369	197	11	color	color	NOUN
eurjchem-1369	197	12	:	:	PUNCT
eurjchem-1369	197	13	yellow	yellow	ADJ
eurjchem-1369	197	14	crystals	crystal	NOUN
eurjchem-1369	197	15	.	.	PUNCT
eurjchem-1369	198	1	yield	yield	NOUN
eurjchem-1369	198	2	:	:	PUNCT
eurjchem-1369	198	3	47	47	NUM
eurjchem-1369	198	4	%	%	NOUN
eurjchem-1369	198	5	.	.	PUNCT
eurjchem-1369	199	1	m.p	m.p	PROPN
eurjchem-1369	199	2	.	.	PROPN
eurjchem-1369	199	3	:	:	PUNCT
eurjchem-1369	200	1	357‐359	357‐359	PROPN
eurjchem-1369	200	2	°	°	SYM
eurjchem-1369	200	3	c	c	X
eurjchem-1369	200	4	.	.	PUNCT
eurjchem-1369	201	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	201	2	(	(	PUNCT
eurjchem-1369	201	3	kbr	kbr	PROPN
eurjchem-1369	201	4	,	,	PUNCT
eurjchem-1369	201	5			PROPN
eurjchem-1369	201	6	,	,	PUNCT
eurjchem-1369	201	7	cm‐1	cm‐1	PROPN
eurjchem-1369	201	8	):	):	PUNCT
eurjchem-1369	201	9	3413‐3213	3413‐3213	NUM
eurjchem-1369	201	10	(	(	PUNCT
eurjchem-1369	201	11	nh2	nh2	PROPN
eurjchem-1369	201	12	and	and	CCONJ
eurjchem-1369	201	13	nh	nh	PROPN
eurjchem-1369	201	14	)	)	PUNCT
eurjchem-1369	201	15	,	,	PUNCT
eurjchem-1369	201	16	2213	2213	NUM
eurjchem-1369	201	17	(	(	PUNCT
eurjchem-1369	201	18	cn	cn	NOUN
eurjchem-1369	201	19	)	)	PUNCT
eurjchem-1369	201	20	,	,	PUNCT
eurjchem-1369	201	21	1700	1700	NUM
eurjchem-1369	201	22	,	,	PUNCT
eurjchem-1369	201	23	1689	1689	NUM
eurjchem-1369	201	24	(	(	PUNCT
eurjchem-1369	201	25	c	c	X
eurjchem-1369	201	26	=	=	SYM
eurjchem-1369	201	27	o	o	NOUN
eurjchem-1369	201	28	's	's	PART
eurjchem-1369	201	29	)	)	PUNCT
eurjchem-1369	201	30	.	.	PUNCT
eurjchem-1369	202	1	1h	1h	NUM
eurjchem-1369	202	2	nmr	nmr	NOUN
eurjchem-1369	202	3	(	(	PUNCT
eurjchem-1369	202	4	250	250	NUM
eurjchem-1369	202	5	mhz	mhz	NOUN
eurjchem-1369	202	6	,	,	PUNCT
eurjchem-1369	202	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	202	8	,	,	PUNCT
eurjchem-1369	202	9	δ	δ	PROPN
eurjchem-1369	202	10	,	,	PUNCT
eurjchem-1369	202	11	ppm	ppm	NUM
eurjchem-1369	202	12	):	):	PUNCT
eurjchem-1369	202	13	1.15‐1.32	1.15‐1.32	NUM
eurjchem-1369	202	14	(	(	PUNCT
eurjchem-1369	202	15	t	t	PROPN
eurjchem-1369	202	16	,	,	PUNCT
eurjchem-1369	202	17	3h	3h	NUM
eurjchem-1369	202	18	,	,	PUNCT
eurjchem-1369	202	19	ch3	ch3	PROPN
eurjchem-1369	202	20	)	)	PUNCT
eurjchem-1369	202	21	,	,	PUNCT
eurjchem-1369	202	22	4.2‐4.35	4.2‐4.35	PROPN
eurjchem-1369	202	23	(	(	PUNCT
eurjchem-1369	202	24	q	q	NOUN
eurjchem-1369	202	25	,	,	PUNCT
eurjchem-1369	202	26	2h	2h	NUM
eurjchem-1369	202	27	,	,	PUNCT
eurjchem-1369	202	28	‐ch2	‐ch2	NUM
eurjchem-1369	202	29	)	)	PUNCT
eurjchem-1369	202	30	,	,	PUNCT
eurjchem-1369	202	31	7.10	7.10	NUM
eurjchem-1369	202	32	(	(	PUNCT
eurjchem-1369	202	33	br.s	br.s	PROPN
eurjchem-1369	202	34	,	,	PUNCT
eurjchem-1369	202	35	2h	2h	NUM
eurjchem-1369	202	36	,	,	PUNCT
eurjchem-1369	202	37	nh2	nh2	PROPN
eurjchem-1369	202	38	)	)	PUNCT
eurjchem-1369	202	39	,	,	PUNCT
eurjchem-1369	202	40	7.88	7.88	NUM
eurjchem-1369	202	41	(	(	PUNCT
eurjchem-1369	202	42	br.s	br.s	PROPN
eurjchem-1369	202	43	,	,	PUNCT
eurjchem-1369	202	44	2h	2h	NUM
eurjchem-1369	202	45	,	,	PUNCT
eurjchem-1369	202	46	nh2	nh2	PROPN
eurjchem-1369	202	47	)	)	PUNCT
eurjchem-1369	202	48	,	,	PUNCT
eurjchem-1369	202	49	8.50	8.50	NUM
eurjchem-1369	202	50	(	(	PUNCT
eurjchem-1369	202	51	s	s	PROPN
eurjchem-1369	202	52	,	,	PUNCT
eurjchem-1369	202	53	1h	1h	NUM
eurjchem-1369	202	54	,	,	PUNCT
eurjchem-1369	202	55	ar‐h	ar‐h	NOUN
eurjchem-1369	202	56	)	)	PUNCT
eurjchem-1369	202	57	,	,	PUNCT
eurjchem-1369	202	58	9.15	9.15	NUM
eurjchem-1369	202	59	(	(	PUNCT
eurjchem-1369	202	60	br.s	br.s	PROPN
eurjchem-1369	202	61	,	,	PUNCT
eurjchem-1369	202	62	1h	1h	NUM
eurjchem-1369	202	63	,	,	PUNCT
eurjchem-1369	202	64	nh	nh	PROPN
eurjchem-1369	202	65	)	)	PUNCT
eurjchem-1369	202	66	.	.	PUNCT
eurjchem-1369	203	1	13c	13c	NOUN
eurjchem-1369	203	2	nmr	nmr	NOUN
eurjchem-1369	203	3	(	(	PUNCT
eurjchem-1369	203	4	75	75	NUM
eurjchem-1369	203	5	mhz	mhz	NOUN
eurjchem-1369	203	6	,	,	PUNCT
eurjchem-1369	203	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	203	8	,	,	PUNCT
eurjchem-1369	203	9	δ	δ	PROPN
eurjchem-1369	203	10	,	,	PUNCT
eurjchem-1369	203	11	ppm	ppm	NUM
eurjchem-1369	203	12	):	):	PUNCT
eurjchem-1369	203	13	19.7	19.7	NUM
eurjchem-1369	203	14	(	(	PUNCT
eurjchem-1369	203	15	1c	1c	NOUN
eurjchem-1369	203	16	,	,	PUNCT
eurjchem-1369	203	17	ch3	ch3	PROPN
eurjchem-1369	203	18	)	)	PUNCT
eurjchem-1369	203	19	,	,	PUNCT
eurjchem-1369	203	20	65.7	65.7	NUM
eurjchem-1369	203	21	(	(	PUNCT
eurjchem-1369	203	22	1c	1c	NOUN
eurjchem-1369	203	23	,	,	PUNCT
eurjchem-1369	203	24	ch2	ch2	PROPN
eurjchem-1369	203	25	)	)	PUNCT
eurjchem-1369	203	26	,	,	PUNCT
eurjchem-1369	203	27	83.00	83.00	NUM
eurjchem-1369	203	28	(	(	PUNCT
eurjchem-1369	203	29	1c	1c	NOUN
eurjchem-1369	203	30	,	,	PUNCT
eurjchem-1369	203	31	=	=	NOUN
eurjchem-1369	203	32	c‐n	c‐n	X
eurjchem-1369	203	33	)	)	PUNCT
eurjchem-1369	203	34	,	,	PUNCT
eurjchem-1369	203	35	93.36	93.36	NUM
eurjchem-1369	203	36	(	(	PUNCT
eurjchem-1369	203	37	1c	1c	NOUN
eurjchem-1369	203	38	,	,	PUNCT
eurjchem-1369	203	39	n	n	CCONJ
eurjchem-1369	203	40	=	=	SYM
eurjchem-1369	203	41	c‐n	c‐n	NOUN
eurjchem-1369	203	42	)	)	PUNCT
eurjchem-1369	203	43	,	,	PUNCT
eurjchem-1369	203	44	120.9	120.9	NUM
eurjchem-1369	203	45	(	(	PUNCT
eurjchem-1369	203	46	1c	1c	NOUN
eurjchem-1369	203	47	,	,	PUNCT
eurjchem-1369	203	48	n	n	CCONJ
eurjchem-1369	203	49	=	=	NOUN
eurjchem-1369	203	50	c‐nh2	c‐nh2	PROPN
eurjchem-1369	203	51	)	)	PUNCT
eurjchem-1369	203	52	,	,	PUNCT
eurjchem-1369	203	53	153.4	153.4	NUM
eurjchem-1369	203	54	(	(	PUNCT
eurjchem-1369	203	55	1c	1c	NOUN
eurjchem-1369	203	56	,	,	PUNCT
eurjchem-1369	203	57	c	c	X
eurjchem-1369	203	58	=	=	SYM
eurjchem-1369	203	59	c‐n	c‐n	NOUN
eurjchem-1369	203	60	)	)	PUNCT
eurjchem-1369	203	61	,	,	PUNCT
eurjchem-1369	203	62	154.3	154.3	NUM
eurjchem-1369	203	63	(	(	PUNCT
eurjchem-1369	203	64	1c	1c	NOUN
eurjchem-1369	203	65	,	,	PUNCT
eurjchem-1369	203	66	=	=	NOUN
eurjchem-1369	203	67	c‐	c‐	NOUN
eurjchem-1369	203	68	cooet	cooet	NOUN
eurjchem-1369	203	69	)	)	PUNCT
eurjchem-1369	203	70	,	,	PUNCT
eurjchem-1369	203	71	158.7	158.7	NUM
eurjchem-1369	203	72	(	(	PUNCT
eurjchem-1369	203	73	1c	1c	NOUN
eurjchem-1369	203	74	,	,	PUNCT
eurjchem-1369	203	75	=	=	NOUN
eurjchem-1369	203	76	c‐cn	c‐cn	NOUN
eurjchem-1369	203	77	)	)	PUNCT
eurjchem-1369	203	78	,	,	PUNCT
eurjchem-1369	203	79	159.5	159.5	NUM
eurjchem-1369	203	80	(	(	PUNCT
eurjchem-1369	203	81	1c	1c	X
eurjchem-1369	203	82	,	,	PUNCT
eurjchem-1369	203	83	cn	cn	PROPN
eurjchem-1369	203	84	)	)	PUNCT
eurjchem-1369	203	85	,	,	PUNCT
eurjchem-1369	203	86	161.5	161.5	NUM
eurjchem-1369	203	87	(	(	PUNCT
eurjchem-1369	203	88	1c	1c	NOUN
eurjchem-1369	203	89	,	,	PUNCT
eurjchem-1369	203	90	conh2	conh2	PROPN
eurjchem-1369	203	91	)	)	PUNCT
eurjchem-1369	203	92	,	,	PUNCT
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eurjchem-1369	203	94	(	(	PUNCT
eurjchem-1369	203	95	1c	1c	NOUN
eurjchem-1369	203	96	,	,	PUNCT
eurjchem-1369	203	97	cooet	cooet	NOUN
eurjchem-1369	203	98	)	)	PUNCT
eurjchem-1369	203	99	.	.	PUNCT
eurjchem-1369	204	1	ms	ms	NOUN
eurjchem-1369	204	2	(	(	PUNCT
eurjchem-1369	204	3	ei	ei	PROPN
eurjchem-1369	204	4	,	,	PUNCT
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eurjchem-1369	204	8	(	(	PUNCT
eurjchem-1369	204	9	%	%	NOUN
eurjchem-1369	204	10	)	)	PUNCT
eurjchem-1369	204	11	):	):	PUNCT
eurjchem-1369	204	12	289	289	NUM
eurjchem-1369	204	13	(	(	PUNCT
eurjchem-1369	204	14	m+	m+	NUM
eurjchem-1369	204	15	,	,	PUNCT
eurjchem-1369	204	16	5	5	NUM
eurjchem-1369	204	17	)	)	PUNCT
eurjchem-1369	204	18	.	.	PUNCT
eurjchem-1369	205	1	anal	anal	PROPN
eurjchem-1369	205	2	.	.	PUNCT
eurjchem-1369	205	3	calcd	calcd	NOUN
eurjchem-1369	205	4	.	.	PUNCT
eurjchem-1369	206	1	for	for	SCONJ
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eurjchem-1369	206	3	:	:	PUNCT
eurjchem-1369	206	4	c	c	X
eurjchem-1369	206	5	,	,	PUNCT
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eurjchem-1369	206	7	;	;	PUNCT
eurjchem-1369	206	8	h	h	NOUN
eurjchem-1369	206	9	,	,	PUNCT
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eurjchem-1369	206	11	;	;	PUNCT
eurjchem-1369	206	12	n	n	CCONJ
eurjchem-1369	206	13	,	,	PUNCT
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eurjchem-1369	206	17	:	:	PUNCT
eurjchem-1369	207	1	c	c	X
eurjchem-1369	207	2	,	,	PUNCT
eurjchem-1369	207	3	45.96	45.96	NUM
eurjchem-1369	207	4	;	;	PUNCT
eurjchem-1369	207	5	h	h	NOUN
eurjchem-1369	207	6	,	,	PUNCT
eurjchem-1369	207	7	3.63	3.63	NUM
eurjchem-1369	207	8	;	;	PUNCT
eurjchem-1369	207	9	n	n	CCONJ
eurjchem-1369	207	10	,	,	PUNCT
eurjchem-1369	207	11	33.91	33.91	NUM
eurjchem-1369	207	12	%	%	NOUN
eurjchem-1369	207	13	.	.	PUNCT
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eurjchem-1369	208	2	,	,	PUNCT
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eurjchem-1369	208	4	xylic	xylic	PROPN
eurjchem-1369	208	5	acid	acid	PROPN
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eurjchem-1369	208	7	ester	ester	NOUN
eurjchem-1369	208	8	(	(	PUNCT
eurjchem-1369	208	9	13b	13b	NUM
eurjchem-1369	208	10	):	):	PUNCT
eurjchem-1369	208	11	color	color	NOUN
eurjchem-1369	208	12	:	:	PUNCT
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eurjchem-1369	208	15	.	.	PUNCT
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eurjchem-1369	209	2	:	:	PUNCT
eurjchem-1369	209	3	51	51	NUM
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eurjchem-1369	209	5	.	.	PUNCT
eurjchem-1369	210	1	m.p	m.p	PROPN
eurjchem-1369	210	2	.	.	PROPN
eurjchem-1369	210	3	:	:	PUNCT
eurjchem-1369	211	1	337‐339	337‐339	PROPN
eurjchem-1369	211	2	°	°	SYM
eurjchem-1369	211	3	c	c	PROPN
eurjchem-1369	211	4	.	.	PUNCT
eurjchem-1369	212	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	212	2	(	(	PUNCT
eurjchem-1369	212	3	kbr	kbr	PROPN
eurjchem-1369	212	4	,	,	PUNCT
eurjchem-1369	212	5			PROPN
eurjchem-1369	212	6	,	,	PUNCT
eurjchem-1369	212	7	cm‐1	cm‐1	PROPN
eurjchem-1369	212	8	):	):	PUNCT
eurjchem-1369	212	9	3345‐3456	3345‐3456	PROPN
eurjchem-1369	212	10	(	(	PUNCT
eurjchem-1369	212	11	nh2	nh2	PROPN
eurjchem-1369	212	12	)	)	PUNCT
eurjchem-1369	212	13	,	,	PUNCT
eurjchem-1369	212	14	3165	3165	NUM
eurjchem-1369	212	15	(	(	PUNCT
eurjchem-1369	212	16	nh	nh	NOUN
eurjchem-1369	212	17	)	)	PUNCT
eurjchem-1369	212	18	,	,	PUNCT
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eurjchem-1369	212	20	,	,	PUNCT
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eurjchem-1369	212	22	(	(	PUNCT
eurjchem-1369	212	23	c	c	X
eurjchem-1369	212	24	=	=	SYM
eurjchem-1369	212	25	o	o	NOUN
eurjchem-1369	212	26	's	's	PART
eurjchem-1369	212	27	)	)	PUNCT
eurjchem-1369	212	28	.	.	PUNCT
eurjchem-1369	213	1	1h	1h	NUM
eurjchem-1369	213	2	nmr	nmr	NOUN
eurjchem-1369	213	3	(	(	PUNCT
eurjchem-1369	213	4	250	250	NUM
eurjchem-1369	213	5	mhz	mhz	NOUN
eurjchem-1369	213	6	,	,	PUNCT
eurjchem-1369	213	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	213	8	,	,	PUNCT
eurjchem-1369	213	9	δ	δ	PROPN
eurjchem-1369	213	10	,	,	PUNCT
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eurjchem-1369	213	12	):	):	PUNCT
eurjchem-1369	213	13	1.21‐1.34	1.21‐1.34	NUM
eurjchem-1369	213	14	(	(	PUNCT
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eurjchem-1369	213	18	,	,	PUNCT
eurjchem-1369	213	19	2ch3	2ch3	NUM
eurjchem-1369	213	20	)	)	PUNCT
eurjchem-1369	213	21	,	,	PUNCT
eurjchem-1369	213	22	4.20‐4.35	4.20‐4.35	NUM
eurjchem-1369	213	23	(	(	PUNCT
eurjchem-1369	213	24	m	m	PROPN
eurjchem-1369	213	25	,	,	PUNCT
eurjchem-1369	213	26	4h	4h	NOUN
eurjchem-1369	213	27	,	,	PUNCT
eurjchem-1369	213	28	2ch2	2ch2	NUM
eurjchem-1369	213	29	)	)	PUNCT
eurjchem-1369	213	30	,	,	PUNCT
eurjchem-1369	213	31	6.65	6.65	NUM
eurjchem-1369	213	32	(	(	PUNCT
eurjchem-1369	213	33	br.s	br.s	PROPN
eurjchem-1369	213	34	,	,	PUNCT
eurjchem-1369	213	35	2h	2h	NUM
eurjchem-1369	213	36	,	,	PUNCT
eurjchem-1369	213	37	nh2	nh2	PROPN
eurjchem-1369	213	38	)	)	PUNCT
eurjchem-1369	213	39	,	,	PUNCT
eurjchem-1369	213	40	8.15	8.15	NUM
eurjchem-1369	213	41	(	(	PUNCT
eurjchem-1369	213	42	br.s	br.s	PROPN
eurjchem-1369	213	43	,	,	PUNCT
eurjchem-1369	213	44	2h	2h	NUM
eurjchem-1369	213	45	,	,	PUNCT
eurjchem-1369	213	46	nh2	nh2	PROPN
eurjchem-1369	213	47	)	)	PUNCT
eurjchem-1369	213	48	,	,	PUNCT
eurjchem-1369	213	49	8.40	8.40	NUM
eurjchem-1369	213	50	(	(	PUNCT
eurjchem-1369	213	51	s	s	PROPN
eurjchem-1369	213	52	,	,	PUNCT
eurjchem-1369	213	53	1h	1h	NUM
eurjchem-1369	213	54	,	,	PUNCT
eurjchem-1369	213	55	ar'h	ar'h	NOUN
eurjchem-1369	213	56	)	)	PUNCT
eurjchem-1369	213	57	,	,	PUNCT
eurjchem-1369	213	58	9.10	9.10	NUM
eurjchem-1369	213	59	(	(	PUNCT
eurjchem-1369	213	60	br.s	br.s	PROPN
eurjchem-1369	213	61	,	,	PUNCT
eurjchem-1369	213	62	1h	1h	NUM
eurjchem-1369	213	63	,	,	PUNCT
eurjchem-1369	213	64	nh	nh	PROPN
eurjchem-1369	213	65	)	)	PUNCT
eurjchem-1369	213	66	.	.	PUNCT
eurjchem-1369	214	1	ms	ms	NOUN
eurjchem-1369	214	2	(	(	PUNCT
eurjchem-1369	214	3	ei	ei	PROPN
eurjchem-1369	214	4	,	,	PUNCT
eurjchem-1369	214	5	m	m	PROPN
eurjchem-1369	214	6	/	/	SYM
eurjchem-1369	214	7	z	z	PROPN
eurjchem-1369	214	8	(	(	PUNCT
eurjchem-1369	214	9	%	%	NOUN
eurjchem-1369	214	10	)	)	PUNCT
eurjchem-1369	214	11	):	):	PUNCT
eurjchem-1369	214	12	336	336	NUM
eurjchem-1369	214	13	(	(	PUNCT
eurjchem-1369	214	14	m+	m+	NUM
eurjchem-1369	214	15	,	,	PUNCT
eurjchem-1369	214	16	22	22	NUM
eurjchem-1369	214	17	)	)	PUNCT
eurjchem-1369	214	18	.	.	PUNCT
eurjchem-1369	215	1	anal	anal	PROPN
eurjchem-1369	215	2	.	.	PUNCT
eurjchem-1369	215	3	calcd	calcd	NOUN
eurjchem-1369	215	4	.	.	PUNCT
eurjchem-1369	216	1	for	for	ADP
eurjchem-1369	216	2	c13h16n6o5	c13h16n6o5	PROPN
eurjchem-1369	216	3	:	:	PUNCT
eurjchem-1369	216	4	c	c	X
eurjchem-1369	216	5	,	,	PUNCT
eurjchem-1369	216	6	46.43	46.43	NUM
eurjchem-1369	216	7	;	;	PUNCT
eurjchem-1369	216	8	h	h	NOUN
eurjchem-1369	216	9	,	,	PUNCT
eurjchem-1369	216	10	4.80	4.80	NUM
eurjchem-1369	216	11	;	;	PUNCT
eurjchem-1369	216	12	n	n	CCONJ
eurjchem-1369	216	13	,	,	PUNCT
eurjchem-1369	216	14	24.99	24.99	NUM
eurjchem-1369	216	15	.	.	PUNCT
eurjchem-1369	216	16	found	find	VERB
eurjchem-1369	216	17	:	:	PUNCT
eurjchem-1369	217	1	c	c	X
eurjchem-1369	217	2	,	,	PUNCT
eurjchem-1369	217	3	46.66	46.66	NUM
eurjchem-1369	217	4	;	;	PUNCT
eurjchem-1369	217	5	h	h	NOUN
eurjchem-1369	217	6	,	,	PUNCT
eurjchem-1369	217	7	4.65	4.65	NUM
eurjchem-1369	217	8	;	;	PUNCT
eurjchem-1369	217	9	n	n	CCONJ
eurjchem-1369	217	10	,	,	PUNCT
eurjchem-1369	217	11	24.80	24.80	NUM
eurjchem-1369	217	12	%	%	NOUN
eurjchem-1369	217	13	.	.	PUNCT
eurjchem-1369	218	1	2.2.7	2.2.7	X
eurjchem-1369	218	2	.	.	PUNCT
eurjchem-1369	219	1	synthesis	synthesis	NOUN
eurjchem-1369	219	2	of	of	ADP
eurjchem-1369	219	3	4‐amino‐2‐methylsulfanyl‐7‐ureido‐pyra	4‐amino‐2‐methylsulfanyl‐7‐ureido‐pyra	PROPN
eurjchem-1369	219	4	zolo[1,5‐a][1,3,5]triazine‐8‐carboxylic	zolo[1,5‐a][1,3,5]triazine‐8‐carboxylic	PROPN
eurjchem-1369	219	5	acid	acid	PROPN
eurjchem-1369	219	6	ethyl	ethyl	PROPN
eurjchem-1369	219	7	ester	ester	NOUN
eurjchem-1369	219	8	(	(	PUNCT
eurjchem-1369	219	9	14	14	NUM
eurjchem-1369	219	10	)	)	PUNCT
eurjchem-1369	219	11	to	to	ADP
eurjchem-1369	219	12	a	a	DET
eurjchem-1369	219	13	solution	solution	NOUN
eurjchem-1369	219	14	of	of	ADP
eurjchem-1369	219	15	compound	compound	NOUN
eurjchem-1369	219	16	4a	4a	NOUN
eurjchem-1369	219	17	(	(	PUNCT
eurjchem-1369	219	18	2.13	2.13	NUM
eurjchem-1369	219	19	g	g	NOUN
eurjchem-1369	219	20	,	,	PUNCT
eurjchem-1369	219	21	0.01	0.01	NUM
eurjchem-1369	219	22	mole	mole	NOUN
eurjchem-1369	219	23	)	)	PUNCT
eurjchem-1369	219	24	in	in	ADP
eurjchem-1369	219	25	(	(	PUNCT
eurjchem-1369	219	26	10	10	NUM
eurjchem-1369	219	27	ml	ml	NOUN
eurjchem-1369	219	28	)	)	PUNCT
eurjchem-1369	219	29	dimethylformamide	dimethylformamide	NOUN
eurjchem-1369	219	30	and	and	CCONJ
eurjchem-1369	219	31	0.5	0.5	NUM
eurjchem-1369	219	32	g	g	NOUN
eurjchem-1369	219	33	potassium	potassium	NOUN
eurjchem-1369	219	34	carbonate	carbonate	NOUN
eurjchem-1369	219	35	,	,	PUNCT
eurjchem-1369	219	36	n‐	n‐	NOUN
eurjchem-1369	219	37	bis(methylthio)methylenecyanamide	bis(methylthio)methylenecyanamide	NUM
eurjchem-1369	219	38	(	(	PUNCT
eurjchem-1369	219	39	1	1	NUM
eurjchem-1369	219	40	)	)	PUNCT
eurjchem-1369	219	41	(	(	PUNCT
eurjchem-1369	219	42	1.46	1.46	NUM
eurjchem-1369	219	43	g	g	NOUN
eurjchem-1369	219	44	,	,	PUNCT
eurjchem-1369	219	45	0.01	0.01	NUM
eurjchem-1369	219	46	mole	mole	NOUN
eurjchem-1369	219	47	)	)	PUNCT
eurjchem-1369	219	48	was	be	AUX
eurjchem-1369	219	49	added	add	VERB
eurjchem-1369	219	50	.	.	PUNCT
eurjchem-1369	220	1	the	the	DET
eurjchem-1369	220	2	reaction	reaction	NOUN
eurjchem-1369	220	3	mixture	mixture	NOUN
eurjchem-1369	220	4	was	be	AUX
eurjchem-1369	220	5	stirred	stir	VERB
eurjchem-1369	220	6	at	at	ADP
eurjchem-1369	220	7	room	room	NOUN
eurjchem-1369	220	8	temperature	temperature	NOUN
eurjchem-1369	220	9	for	for	ADP
eurjchem-1369	220	10	6bh	6bh	NOUN
eurjchem-1369	220	11	.	.	PUNCT
eurjchem-1369	221	1	after	after	ADP
eurjchem-1369	221	2	this	this	DET
eurjchem-1369	221	3	time	time	NOUN
eurjchem-1369	221	4	the	the	DET
eurjchem-1369	221	5	reaction	reaction	NOUN
eurjchem-1369	221	6	mixture	mixture	NOUN
eurjchem-1369	221	7	was	be	AUX
eurjchem-1369	221	8	acidified	acidify	VERB
eurjchem-1369	221	9	with	with	ADP
eurjchem-1369	221	10	10	10	NUM
eurjchem-1369	221	11	%	%	NOUN
eurjchem-1369	221	12	hydrochloric	hydrochloric	ADJ
eurjchem-1369	221	13	acid	acid	NOUN
eurjchem-1369	221	14	.	.	PUNCT
eurjchem-1369	222	1	the	the	DET
eurjchem-1369	222	2	precipitate	precipitate	NOUN
eurjchem-1369	222	3	that	that	PRON
eurjchem-1369	222	4	appeared	appear	VERB
eurjchem-1369	222	5	was	be	AUX
eurjchem-1369	222	6	collected	collect	VERB
eurjchem-1369	222	7	by	by	ADP
eurjchem-1369	222	8	filtration	filtration	NOUN
eurjchem-1369	222	9	and	and	CCONJ
eurjchem-1369	222	10	crystallized	crystallize	VERB
eurjchem-1369	222	11	from	from	ADP
eurjchem-1369	222	12	dimethylformamide	dimethylformamide	NOUN
eurjchem-1369	222	13	(	(	PUNCT
eurjchem-1369	222	14	scheme	scheme	NOUN
eurjchem-1369	222	15	4	4	NUM
eurjchem-1369	222	16	)	)	PUNCT
eurjchem-1369	222	17	.	.	PUNCT
eurjchem-1369	223	1	color	color	NOUN
eurjchem-1369	223	2	:	:	PUNCT
eurjchem-1369	223	3	yellow	yellow	ADJ
eurjchem-1369	223	4	crystals	crystal	NOUN
eurjchem-1369	223	5	.	.	PUNCT
eurjchem-1369	224	1	yield	yield	NOUN
eurjchem-1369	224	2	:	:	PUNCT
eurjchem-1369	224	3	66	66	NUM
eurjchem-1369	224	4	%	%	NOUN
eurjchem-1369	224	5	.	.	PUNCT
eurjchem-1369	225	1	m.p	m.p	PROPN
eurjchem-1369	225	2	.	.	PROPN
eurjchem-1369	225	3	:	:	PUNCT
eurjchem-1369	226	1	357‐358	357‐358	NOUN
eurjchem-1369	226	2	°	°	SYM
eurjchem-1369	226	3	c	c	PROPN
eurjchem-1369	226	4	.	.	PUNCT
eurjchem-1369	227	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	227	2	(	(	PUNCT
eurjchem-1369	227	3	kbr	kbr	PROPN
eurjchem-1369	227	4	,	,	PUNCT
eurjchem-1369	227	5			PROPN
eurjchem-1369	227	6	,	,	PUNCT
eurjchem-1369	227	7	cm‐1	cm‐1	PROPN
eurjchem-1369	227	8	):	):	PUNCT
eurjchem-1369	227	9	3325‐3436	3325‐3436	NUM
eurjchem-1369	227	10	(	(	PUNCT
eurjchem-1369	227	11	nh2	nh2	PROPN
eurjchem-1369	227	12	)	)	PUNCT
eurjchem-1369	227	13	,	,	PUNCT
eurjchem-1369	227	14	3277	3277	NUM
eurjchem-1369	227	15	(	(	PUNCT
eurjchem-1369	227	16	nh	nh	NOUN
eurjchem-1369	227	17	)	)	PUNCT
eurjchem-1369	227	18	,	,	PUNCT
eurjchem-1369	227	19	1722	1722	NUM
eurjchem-1369	227	20	,	,	PUNCT
eurjchem-1369	227	21	1684	1684	NUM
eurjchem-1369	227	22	(	(	PUNCT
eurjchem-1369	227	23	c	c	X
eurjchem-1369	227	24	=	=	SYM
eurjchem-1369	227	25	o	o	NOUN
eurjchem-1369	227	26	's	's	PART
eurjchem-1369	227	27	)	)	PUNCT
eurjchem-1369	227	28	.	.	PUNCT
eurjchem-1369	228	1	1h	1h	NUM
eurjchem-1369	228	2	nmr	nmr	NOUN
eurjchem-1369	228	3	(	(	PUNCT
eurjchem-1369	228	4	250	250	NUM
eurjchem-1369	228	5	mhz	mhz	NOUN
eurjchem-1369	228	6	,	,	PUNCT
eurjchem-1369	228	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	228	8	,	,	PUNCT
eurjchem-1369	228	9	δ	δ	PROPN
eurjchem-1369	228	10	,	,	PUNCT
eurjchem-1369	228	11	ppm	ppm	NUM
eurjchem-1369	228	12	):	):	PUNCT
eurjchem-1369	228	13	1.15‐1.32	1.15‐1.32	NUM
eurjchem-1369	228	14	(	(	PUNCT
eurjchem-1369	228	15	t	t	PROPN
eurjchem-1369	228	16	,	,	PUNCT
eurjchem-1369	228	17	3h	3h	NUM
eurjchem-1369	228	18	,	,	PUNCT
eurjchem-1369	228	19	ch3	ch3	PROPN
eurjchem-1369	228	20	)	)	PUNCT
eurjchem-1369	228	21	,	,	PUNCT
eurjchem-1369	228	22	2.40	2.40	NUM
eurjchem-1369	228	23	(	(	PUNCT
eurjchem-1369	228	24	s	s	PROPN
eurjchem-1369	228	25	,	,	PUNCT
eurjchem-1369	228	26	2h	2h	NUM
eurjchem-1369	228	27	,	,	PUNCT
eurjchem-1369	228	28	nh2	nh2	PROPN
eurjchem-1369	228	29	)	)	PUNCT
eurjchem-1369	228	30	,	,	PUNCT
eurjchem-1369	228	31	2.46	2.46	NUM
eurjchem-1369	228	32	(	(	PUNCT
eurjchem-1369	228	33	s	s	PROPN
eurjchem-1369	228	34	,	,	PUNCT
eurjchem-1369	228	35	3h	3h	NUM
eurjchem-1369	228	36	,	,	PUNCT
eurjchem-1369	228	37	sme	sme	NOUN
eurjchem-1369	228	38	)	)	PUNCT
eurjchem-1369	228	39	,	,	PUNCT
eurjchem-1369	228	40	4.20‐4.30	4.20‐4.30	NUM
eurjchem-1369	228	41	(	(	PUNCT
eurjchem-1369	228	42	q	q	NOUN
eurjchem-1369	228	43	,	,	PUNCT
eurjchem-1369	228	44	2h	2h	NUM
eurjchem-1369	228	45	,	,	PUNCT
eurjchem-1369	228	46	‐ch2	‐ch2	NUM
eurjchem-1369	228	47	)	)	PUNCT
eurjchem-1369	228	48	,	,	PUNCT
eurjchem-1369	228	49	7.25	7.25	NUM
eurjchem-1369	228	50	(	(	PUNCT
eurjchem-1369	228	51	s	s	PROPN
eurjchem-1369	228	52	,	,	PUNCT
eurjchem-1369	228	53	2h	2h	NUM
eurjchem-1369	228	54	,	,	PUNCT
eurjchem-1369	228	55	nh2	nh2	PROPN
eurjchem-1369	228	56	)	)	PUNCT
eurjchem-1369	228	57	,	,	PUNCT
eurjchem-1369	228	58	8.7	8.7	NUM
eurjchem-1369	228	59	(	(	PUNCT
eurjchem-1369	228	60	s	s	PROPN
eurjchem-1369	228	61	,	,	PUNCT
eurjchem-1369	228	62	1h	1h	NUM
eurjchem-1369	228	63	,	,	PUNCT
eurjchem-1369	228	64	nh	nh	PROPN
eurjchem-1369	228	65	)	)	PUNCT
eurjchem-1369	228	66	.	.	PUNCT
eurjchem-1369	229	1	ms	ms	NOUN
eurjchem-1369	229	2	(	(	PUNCT
eurjchem-1369	229	3	ei	ei	PROPN
eurjchem-1369	229	4	,	,	PUNCT
eurjchem-1369	229	5	m	m	PROPN
eurjchem-1369	229	6	/	/	SYM
eurjchem-1369	229	7	z	z	PROPN
eurjchem-1369	229	8	(	(	PUNCT
eurjchem-1369	229	9	%	%	NOUN
eurjchem-1369	229	10	)	)	PUNCT
eurjchem-1369	229	11	):	):	PUNCT
eurjchem-1369	229	12	311	311	NUM
eurjchem-1369	229	13	(	(	PUNCT
eurjchem-1369	229	14	m+	m+	NUM
eurjchem-1369	229	15	,	,	PUNCT
eurjchem-1369	229	16	32	32	NUM
eurjchem-1369	229	17	)	)	PUNCT
eurjchem-1369	229	18	.	.	PUNCT
eurjchem-1369	230	1	anal	anal	PROPN
eurjchem-1369	230	2	.	.	PUNCT
eurjchem-1369	230	3	calcd	calcd	NOUN
eurjchem-1369	230	4	.	.	PUNCT
eurjchem-1369	231	1	for	for	SCONJ
eurjchem-1369	231	2	c10h13n7o3s	c10h13n7o3s	NUM
eurjchem-1369	231	3	:	:	PUNCT
eurjchem-1369	231	4	c	c	X
eurjchem-1369	231	5	,	,	PUNCT
eurjchem-1369	231	6	38.58	38.58	NUM
eurjchem-1369	231	7	;	;	PUNCT
eurjchem-1369	231	8	h	h	NOUN
eurjchem-1369	231	9	,	,	PUNCT
eurjchem-1369	231	10	4.21	4.21	NUM
eurjchem-1369	231	11	;	;	PUNCT
eurjchem-1369	231	12	n	n	CCONJ
eurjchem-1369	231	13	,	,	PUNCT
eurjchem-1369	231	14	31.49	31.49	NUM
eurjchem-1369	231	15	.	.	PUNCT
eurjchem-1369	231	16	found	find	VERB
eurjchem-1369	231	17	:	:	PUNCT
eurjchem-1369	232	1	c	c	X
eurjchem-1369	232	2	,	,	PUNCT
eurjchem-1369	232	3	38.86	38.86	NUM
eurjchem-1369	232	4	;	;	PUNCT
eurjchem-1369	233	1	h	h	NOUN
eurjchem-1369	233	2	,	,	PUNCT
eurjchem-1369	233	3	4.53	4.53	NUM
eurjchem-1369	233	4	;	;	PUNCT
eurjchem-1369	233	5	n	n	CCONJ
eurjchem-1369	233	6	,	,	PUNCT
eurjchem-1369	233	7	31.61	31.61	NUM
eurjchem-1369	233	8	%	%	NOUN
eurjchem-1369	233	9	.	.	PUNCT
eurjchem-1369	234	1	2.2.8	2.2.8	X
eurjchem-1369	234	2	.	.	PUNCT
eurjchem-1369	235	1	synthesis	synthesis	NOUN
eurjchem-1369	235	2	of	of	ADP
eurjchem-1369	235	3	5‐[(2‐hydroxy‐benzylidene)amino]‐3‐	5‐[(2‐hydroxy‐benzylidene)amino]‐3‐	NUM
eurjchem-1369	235	4	ureido‐1h‐pyrazolo‐4‐carboxylic	ureido‐1h‐pyrazolo‐4‐carboxylic	ADJ
eurjchem-1369	235	5	acid	acid	NOUN
eurjchem-1369	235	6	ethyl	ethyl	PROPN
eurjchem-1369	235	7	ester	ester	NOUN
eurjchem-1369	235	8	(	(	PUNCT
eurjchem-1369	235	9	15	15	NUM
eurjchem-1369	235	10	)	)	PUNCT
eurjchem-1369	235	11	to	to	ADP
eurjchem-1369	235	12	a	a	DET
eurjchem-1369	235	13	solution	solution	NOUN
eurjchem-1369	235	14	of	of	ADP
eurjchem-1369	235	15	compound	compound	NOUN
eurjchem-1369	235	16	4a	4a	NOUN
eurjchem-1369	235	17	(	(	PUNCT
eurjchem-1369	235	18	2.13	2.13	NUM
eurjchem-1369	235	19	g	g	NOUN
eurjchem-1369	235	20	,	,	PUNCT
eurjchem-1369	235	21	0.01	0.01	NUM
eurjchem-1369	235	22	mole	mole	NOUN
eurjchem-1369	235	23	)	)	PUNCT
eurjchem-1369	235	24	in	in	ADP
eurjchem-1369	235	25	(	(	PUNCT
eurjchem-1369	235	26	10	10	NUM
eurjchem-1369	235	27	ml	ml	NOUN
eurjchem-1369	235	28	)	)	PUNCT
eurjchem-1369	235	29	ethanol	ethanol	NOUN
eurjchem-1369	235	30	and	and	CCONJ
eurjchem-1369	235	31	(	(	PUNCT
eurjchem-1369	235	32	0.1	0.1	NUM
eurjchem-1369	235	33	ml	ml	NOUN
eurjchem-1369	235	34	)	)	PUNCT
eurjchem-1369	235	35	piperidine	piperidine	NOUN
eurjchem-1369	235	36	,	,	PUNCT
eurjchem-1369	235	37	2‐hydroxybenzaldehyde	2‐hydroxybenzaldehyde	NUM
eurjchem-1369	235	38	(	(	PUNCT
eurjchem-1369	235	39	1.2	1.2	NUM
eurjchem-1369	235	40	g	g	NOUN
eurjchem-1369	235	41	,	,	PUNCT
eurjchem-1369	235	42	0.01	0.01	NUM
eurjchem-1369	235	43	mole	mole	NOUN
eurjchem-1369	235	44	)	)	PUNCT
eurjchem-1369	235	45	was	be	AUX
eurjchem-1369	235	46	added	add	VERB
eurjchem-1369	235	47	.	.	PUNCT
eurjchem-1369	236	1	the	the	DET
eurjchem-1369	236	2	reaction	reaction	NOUN
eurjchem-1369	236	3	mixture	mixture	NOUN
eurjchem-1369	236	4	was	be	AUX
eurjchem-1369	236	5	refluxed	refluxe	VERB
eurjchem-1369	236	6	for	for	ADP
eurjchem-1369	236	7	2	2	NUM
eurjchem-1369	236	8	h	h	NOUN
eurjchem-1369	236	9	,	,	PUNCT
eurjchem-1369	236	10	and	and	CCONJ
eurjchem-1369	236	11	the	the	DET
eurjchem-1369	236	12	obtained	obtain	VERB
eurjchem-1369	236	13	product	product	NOUN
eurjchem-1369	236	14	was	be	AUX
eurjchem-1369	236	15	crystallized	crystallize	VERB
eurjchem-1369	236	16	from	from	ADP
eurjchem-1369	236	17	chloroform	chloroform	NOUN
eurjchem-1369	236	18	(	(	PUNCT
eurjchem-1369	236	19	scheme	scheme	NOUN
eurjchem-1369	236	20	4	4	NUM
eurjchem-1369	236	21	)	)	PUNCT
eurjchem-1369	236	22	.	.	PUNCT
eurjchem-1369	237	1	color	color	NOUN
eurjchem-1369	237	2	:	:	PUNCT
eurjchem-1369	237	3	yellow	yellow	ADJ
eurjchem-1369	237	4	crystals	crystal	NOUN
eurjchem-1369	237	5	.	.	PUNCT
eurjchem-1369	238	1	yield	yield	NOUN
eurjchem-1369	238	2	:	:	PUNCT
eurjchem-1369	238	3	78	78	NUM
eurjchem-1369	238	4	%	%	NOUN
eurjchem-1369	238	5	.	.	PUNCT
eurjchem-1369	239	1	m.p	m.p	PROPN
eurjchem-1369	239	2	.	.	PROPN
eurjchem-1369	239	3	:	:	PUNCT
eurjchem-1369	240	1	279‐380	279‐380	NUM
eurjchem-1369	240	2	°	°	ADP
eurjchem-1369	240	3	c	c	NOUN
eurjchem-1369	240	4	.	.	PUNCT
eurjchem-1369	240	5	ft‐ir	ft‐ir	NOUN
eurjchem-1369	240	6	(	(	PUNCT
eurjchem-1369	240	7	kbr	kbr	PROPN
eurjchem-1369	240	8	,	,	PUNCT
eurjchem-1369	240	9			PROPN
eurjchem-1369	240	10	,	,	PUNCT
eurjchem-1369	240	11	cm‐1	cm‐1	PROPN
eurjchem-1369	240	12	):	):	PUNCT
eurjchem-1369	240	13	3345‐3456	3345‐3456	PROPN
eurjchem-1369	240	14	(	(	PUNCT
eurjchem-1369	240	15	nh2	nh2	NOUN
eurjchem-1369	240	16	and	and	CCONJ
eurjchem-1369	240	17	oh	oh	INTJ
eurjchem-1369	240	18	)	)	PUNCT
eurjchem-1369	240	19	,	,	PUNCT
eurjchem-1369	240	20	3165	3165	NUM
eurjchem-1369	240	21	(	(	PUNCT
eurjchem-1369	240	22	nh	nh	NOUN
eurjchem-1369	240	23	)	)	PUNCT
eurjchem-1369	240	24	,	,	PUNCT
eurjchem-1369	240	25	1722	1722	NUM
eurjchem-1369	240	26	,	,	PUNCT
eurjchem-1369	240	27	1682	1682	NUM
eurjchem-1369	240	28	(	(	PUNCT
eurjchem-1369	240	29	c	c	X
eurjchem-1369	240	30	=	=	SYM
eurjchem-1369	240	31	o	o	NOUN
eurjchem-1369	240	32	's	's	PART
eurjchem-1369	240	33	)	)	PUNCT
eurjchem-1369	240	34	.	.	PUNCT
eurjchem-1369	241	1	1h	1h	NUM
eurjchem-1369	241	2	nmr	nmr	NOUN
eurjchem-1369	241	3	(	(	PUNCT
eurjchem-1369	241	4	250	250	NUM
eurjchem-1369	241	5	mhz	mhz	NOUN
eurjchem-1369	241	6	,	,	PUNCT
eurjchem-1369	241	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	241	8	,	,	PUNCT
eurjchem-1369	241	9	δ	δ	PROPN
eurjchem-1369	241	10	,	,	PUNCT
eurjchem-1369	241	11	ppm	ppm	NUM
eurjchem-1369	241	12	):	):	PUNCT
eurjchem-1369	241	13	1.15‐1.35	1.15‐1.35	NUM
eurjchem-1369	241	14	(	(	PUNCT
eurjchem-1369	241	15	t	t	PROPN
eurjchem-1369	241	16	,	,	PUNCT
eurjchem-1369	241	17	3h	3h	NUM
eurjchem-1369	241	18	,	,	PUNCT
eurjchem-1369	241	19	ch3	ch3	PROPN
eurjchem-1369	241	20	)	)	PUNCT
eurjchem-1369	241	21	,	,	PUNCT
eurjchem-1369	241	22	3.67	3.67	NUM
eurjchem-1369	241	23	(	(	PUNCT
eurjchem-1369	241	24	s	s	PROPN
eurjchem-1369	241	25	,	,	PUNCT
eurjchem-1369	241	26	1h	1h	NUM
eurjchem-1369	241	27	,	,	PUNCT
eurjchem-1369	241	28	pyrazole‐	pyrazole‐	NOUN
eurjchem-1369	241	29	nh	nh	PROPN
eurjchem-1369	241	30	)	)	PUNCT
eurjchem-1369	241	31	,	,	PUNCT
eurjchem-1369	241	32	4.20‐4.30	4.20‐4.30	NUM
eurjchem-1369	241	33	(	(	PUNCT
eurjchem-1369	241	34	q	q	NOUN
eurjchem-1369	241	35	,	,	PUNCT
eurjchem-1369	241	36	2h	2h	NUM
eurjchem-1369	241	37	,	,	PUNCT
eurjchem-1369	241	38	‐ch2	‐ch2	NUM
eurjchem-1369	241	39	)	)	PUNCT
eurjchem-1369	241	40	,	,	PUNCT
eurjchem-1369	241	41	6.65	6.65	NUM
eurjchem-1369	241	42	(	(	PUNCT
eurjchem-1369	241	43	s	s	NOUN
eurjchem-1369	241	44	,	,	PUNCT
eurjchem-1369	241	45	2h	2h	NUM
eurjchem-1369	241	46	,	,	PUNCT
eurjchem-1369	241	47	nh2	nh2	PROPN
eurjchem-1369	241	48	)	)	PUNCT
eurjchem-1369	241	49	,	,	PUNCT
eurjchem-1369	241	50	7.35‐8.25	7.35‐8.25	NUM
eurjchem-1369	241	51	(	(	PUNCT
eurjchem-1369	241	52	m	m	PROPN
eurjchem-1369	241	53	,	,	PUNCT
eurjchem-1369	241	54	4h	4h	NOUN
eurjchem-1369	241	55	,	,	PUNCT
eurjchem-1369	241	56	ar‐h	ar‐h	PROPN
eurjchem-1369	241	57	)	)	PUNCT
eurjchem-1369	241	58	,	,	PUNCT
eurjchem-1369	241	59	8.2	8.2	NUM
eurjchem-1369	241	60	(	(	PUNCT
eurjchem-1369	241	61	s	s	PROPN
eurjchem-1369	241	62	,	,	PUNCT
eurjchem-1369	241	63	1h	1h	NUM
eurjchem-1369	241	64	,	,	PUNCT
eurjchem-1369	241	65	ch‐benzylideneimin	ch‐benzylideneimin	NOUN
eurjchem-1369	241	66	)	)	PUNCT
eurjchem-1369	241	67	,	,	PUNCT
eurjchem-1369	241	68	10.65	10.65	NUM
eurjchem-1369	241	69	(	(	PUNCT
eurjchem-1369	241	70	s	s	PROPN
eurjchem-1369	241	71	,	,	PUNCT
eurjchem-1369	241	72	1h	1h	NUM
eurjchem-1369	241	73	,	,	PUNCT
eurjchem-1369	241	74	nh	nh	PROPN
eurjchem-1369	241	75	)	)	PUNCT
eurjchem-1369	241	76	,	,	PUNCT
eurjchem-1369	241	77	12.7	12.7	NUM
eurjchem-1369	241	78	(	(	PUNCT
eurjchem-1369	241	79	br.s	br.s	PROPN
eurjchem-1369	241	80	,	,	PUNCT
eurjchem-1369	241	81	1h	1h	NUM
eurjchem-1369	241	82	,	,	PUNCT
eurjchem-1369	241	83	oh	oh	INTJ
eurjchem-1369	241	84	)	)	PUNCT
eurjchem-1369	241	85	.	.	PUNCT
eurjchem-1369	242	1	ms	ms	NOUN
eurjchem-1369	242	2	(	(	PUNCT
eurjchem-1369	242	3	ei	ei	PROPN
eurjchem-1369	242	4	,	,	PUNCT
eurjchem-1369	242	5	m	m	PROPN
eurjchem-1369	242	6	/	/	SYM
eurjchem-1369	242	7	z	z	PROPN
eurjchem-1369	242	8	(	(	PUNCT
eurjchem-1369	242	9	%	%	NOUN
eurjchem-1369	242	10	)	)	PUNCT
eurjchem-1369	242	11	):	):	PUNCT
eurjchem-1369	242	12	317	317	NUM
eurjchem-1369	242	13	(	(	PUNCT
eurjchem-1369	242	14	m+	m+	NUM
eurjchem-1369	242	15	,	,	PUNCT
eurjchem-1369	242	16	100	100	NUM
eurjchem-1369	242	17	)	)	PUNCT
eurjchem-1369	242	18	.	.	PUNCT
eurjchem-1369	243	1	anal	anal	PROPN
eurjchem-1369	243	2	.	.	PUNCT
eurjchem-1369	243	3	calcd	calcd	NOUN
eurjchem-1369	243	4	.	.	PUNCT
eurjchem-1369	244	1	for	for	ADP
eurjchem-1369	244	2	c14h15n5o4	c14h15n5o4	PROPN
eurjchem-1369	244	3	:	:	PUNCT
eurjchem-1369	244	4	c	c	NOUN
eurjchem-1369	244	5	,	,	PUNCT
eurjchem-1369	244	6	52.99	52.99	NUM
eurjchem-1369	244	7	;	;	PUNCT
eurjchem-1369	244	8	h	h	NOUN
eurjchem-1369	244	9	,	,	PUNCT
eurjchem-1369	244	10	4.76	4.76	NUM
eurjchem-1369	244	11	;	;	PUNCT
eurjchem-1369	244	12	n	n	CCONJ
eurjchem-1369	244	13	,	,	PUNCT
eurjchem-1369	244	14	22.07	22.07	NUM
eurjchem-1369	244	15	.	.	PUNCT
eurjchem-1369	244	16	found	find	VERB
eurjchem-1369	244	17	:	:	PUNCT
eurjchem-1369	245	1	c	c	X
eurjchem-1369	245	2	,	,	PUNCT
eurjchem-1369	245	3	52.85	52.85	NUM
eurjchem-1369	245	4	;	;	PUNCT
eurjchem-1369	245	5	h	h	NOUN
eurjchem-1369	245	6	,	,	PUNCT
eurjchem-1369	245	7	4.65	4.65	NUM
eurjchem-1369	245	8	;	;	PUNCT
eurjchem-1369	245	9	n	n	CCONJ
eurjchem-1369	245	10	,	,	PUNCT
eurjchem-1369	245	11	22.32	22.32	NUM
eurjchem-1369	245	12	%	%	NOUN
eurjchem-1369	245	13	.	.	PUNCT
eurjchem-1369	246	1	2.2.9	2.2.9	X
eurjchem-1369	246	2	.	.	PUNCT
eurjchem-1369	247	1	synthesis	synthesis	NOUN
eurjchem-1369	247	2	of	of	ADP
eurjchem-1369	247	3	2‐ureido‐pyrazolo[1,5‐a]quinazoline‐3‐	2‐ureido‐pyrazolo[1,5‐a]quinazoline‐3‐	NUM
eurjchem-1369	247	4	carboxylic	carboxylic	ADJ
eurjchem-1369	247	5	acid	acid	NOUN
eurjchem-1369	247	6	ethyl	ethyl	PROPN
eurjchem-1369	247	7	ester	ester	NOUN
eurjchem-1369	247	8	(	(	PUNCT
eurjchem-1369	247	9	16	16	NUM
eurjchem-1369	247	10	)	)	PUNCT
eurjchem-1369	247	11	to	to	ADP
eurjchem-1369	247	12	a	a	DET
eurjchem-1369	247	13	solution	solution	NOUN
eurjchem-1369	247	14	of	of	ADP
eurjchem-1369	247	15	compound	compound	NOUN
eurjchem-1369	247	16	15	15	NUM
eurjchem-1369	247	17	(	(	PUNCT
eurjchem-1369	247	18	3.17	3.17	NUM
eurjchem-1369	247	19	g	g	NOUN
eurjchem-1369	247	20	,	,	PUNCT
eurjchem-1369	247	21	0.01	0.01	NUM
eurjchem-1369	247	22	mole	mole	NOUN
eurjchem-1369	247	23	)	)	PUNCT
eurjchem-1369	247	24	in	in	ADP
eurjchem-1369	247	25	acetic	acetic	ADJ
eurjchem-1369	247	26	acid	acid	NOUN
eurjchem-1369	247	27	(	(	PUNCT
eurjchem-1369	247	28	20	20	NUM
eurjchem-1369	247	29	ml	ml	NOUN
eurjchem-1369	247	30	)	)	PUNCT
eurjchem-1369	247	31	was	be	AUX
eurjchem-1369	247	32	heated	heat	VERB
eurjchem-1369	247	33	under	under	ADP
eurjchem-1369	247	34	reflux	reflux	NOUN
eurjchem-1369	247	35	for	for	ADP
eurjchem-1369	247	36	4	4	NUM
eurjchem-1369	247	37	h.	h.	PROPN
eurjchem-1369	247	38	abbas‐temirek	abbas‐temirek	PROPN
eurjchem-1369	247	39	and	and	CCONJ
eurjchem-1369	247	40	abo‐bakr	abo‐bakr	ADJ
eurjchem-1369	247	41	/	/	SYM
eurjchem-1369	247	42	european	european	ADJ
eurjchem-1369	247	43	journal	journal	PROPN
eurjchem-1369	247	44	of	of	ADP
eurjchem-1369	247	45	chemistry	chemistry	NOUN
eurjchem-1369	247	46	7	7	NUM
eurjchem-1369	247	47	(	(	PUNCT
eurjchem-1369	247	48	1	1	NUM
eurjchem-1369	247	49	)	)	PUNCT
eurjchem-1369	247	50	(	(	PUNCT
eurjchem-1369	247	51	2016	2016	NUM
eurjchem-1369	247	52	)	)	PUNCT
eurjchem-1369	247	53	107‐114	107‐114	NUM
eurjchem-1369	247	54	111	111	NUM
eurjchem-1369	247	55	n	n	PROPN
eurjchem-1369	247	56	n	n	PRON
eurjchem-1369	247	57	etooc	etooc	NOUN
eurjchem-1369	247	58	nh	nh	PROPN
eurjchem-1369	248	1	n	n	PROPN
eurjchem-1369	248	2	nh2	nh2	PROPN
eurjchem-1369	248	3	ch2n	ch2n	PROPN
eurjchem-1369	248	4	o	o	NOUN
eurjchem-1369	248	5	n	n	CCONJ
eurjchem-1369	248	6	n	n	CCONJ
eurjchem-1369	248	7	cooet	cooet	VERB
eurjchem-1369	248	8	nh	nh	PROPN
eurjchem-1369	248	9	n	n	ADV
eurjchem-1369	248	10	c	c	PROPN
eurjchem-1369	248	11	nh2	nh2	PROPN
eurjchem-1369	248	12	o	o	PROPN
eurjchem-1369	248	13	n	n	CCONJ
eurjchem-1369	248	14	n	n	ADV
eurjchem-1369	248	15	etooc	etooc	NOUN
eurjchem-1369	248	16	nh	nh	PROPN
eurjchem-1369	248	17	n	n	CCONJ
eurjchem-1369	248	18	n	n	PRON
eurjchem-1369	248	19	nh2	nh2	PROPN
eurjchem-1369	248	20	ch2n	ch2n	PROPN
eurjchem-1369	248	21	o	o	PROPN
eurjchem-1369	248	22	rn	rn	PROPN
eurjchem-1369	248	23	nh	nh	PROPN
eurjchem-1369	248	24	cooet	cooet	PROPN
eurjchem-1369	248	25	nh	nh	PROPN
eurjchem-1369	249	1	n	n	PROPN
eurjchem-1369	249	2	c	c	PROPN
eurjchem-1369	249	3	nh2	nh2	PROPN
eurjchem-1369	249	4	o	o	NOUN
eurjchem-1369	250	1	oh	oh	INTJ
eurjchem-1369	250	2	4a	4a	X
eurjchem-1369	250	3	(	(	PUNCT
eurjchem-1369	250	4	1	1	X
eurjchem-1369	250	5	)	)	PUNCT
eurjchem-1369	250	6	r	r	NOUN
eurjchem-1369	250	7	cn	cn	PROPN
eurjchem-1369	250	8	eto	eto	PROPN
eurjchem-1369	250	9	acoh	acoh	PROPN
eurjchem-1369	250	10	13a	13a	PROPN
eurjchem-1369	250	11	,	,	PUNCT
eurjchem-1369	250	12	b	b	PROPN
eurjchem-1369	250	13	14	14	NUM
eurjchem-1369	250	14	16	16	NUM
eurjchem-1369	250	15	15	15	NUM
eurjchem-1369	250	16	ohc	ohc	NOUN
eurjchem-1369	250	17	oh	oh	INTJ
eurjchem-1369	250	18	a	a	NOUN
eurjchem-1369	250	19	;	;	PUNCT
eurjchem-1369	250	20	r	r	NOUN
eurjchem-1369	250	21	=	=	SYM
eurjchem-1369	250	22	cn	cn	PROPN
eurjchem-1369	250	23	,	,	PUNCT
eurjchem-1369	250	24	b	b	NOUN
eurjchem-1369	250	25	;	;	PUNCT
eurjchem-1369	250	26	r	r	NOUN
eurjchem-1369	250	27	=	=	PUNCT
eurjchem-1369	250	28	co2et	co2et	VERB
eurjchem-1369	250	29	k2co3	k2co3	ADJ
eurjchem-1369	250	30	/	/	SYM
eurjchem-1369	250	31	dmf	dmf	PROPN
eurjchem-1369	250	32	etoh	etoh	NOUN
eurjchem-1369	250	33	acoh	acoh	NOUN
eurjchem-1369	250	34	n	n	PROPN
eurjchem-1369	250	35	nh	nh	PROPN
eurjchem-1369	250	36	etooc	etooc	PROPN
eurjchem-1369	250	37	nh	nh	PROPN
eurjchem-1369	250	38	nh2	nh2	PROPN
eurjchem-1369	250	39	c	c	PROPN
eurjchem-1369	250	40	nh2o	nh2o	PROPN
eurjchem-1369	250	41	sch3	sch3	PROPN
eurjchem-1369	250	42	scheme	scheme	NOUN
eurjchem-1369	250	43	4	4	NUM
eurjchem-1369	250	44	the	the	DET
eurjchem-1369	250	45	solvent	solvent	NOUN
eurjchem-1369	250	46	was	be	AUX
eurjchem-1369	250	47	then	then	ADV
eurjchem-1369	250	48	evaporated	evaporate	VERB
eurjchem-1369	250	49	under	under	ADP
eurjchem-1369	250	50	vacuo	vacuo	NOUN
eurjchem-1369	250	51	,	,	PUNCT
eurjchem-1369	250	52	and	and	CCONJ
eurjchem-1369	250	53	the	the	DET
eurjchem-1369	250	54	remaining	remain	VERB
eurjchem-1369	250	55	solid	solid	ADJ
eurjchem-1369	250	56	product	product	NOUN
eurjchem-1369	250	57	was	be	AUX
eurjchem-1369	250	58	crystallized	crystallize	VERB
eurjchem-1369	250	59	from	from	ADP
eurjchem-1369	250	60	dimethyl	dimethyl	PROPN
eurjchem-1369	250	61	formamide	formamide	ADV
eurjchem-1369	250	62	(	(	PUNCT
eurjchem-1369	250	63	scheme	scheme	NOUN
eurjchem-1369	250	64	4	4	NUM
eurjchem-1369	250	65	)	)	PUNCT
eurjchem-1369	250	66	.	.	PUNCT
eurjchem-1369	251	1	color	color	NOUN
eurjchem-1369	251	2	:	:	PUNCT
eurjchem-1369	251	3	red	red	ADJ
eurjchem-1369	251	4	crystals	crystal	NOUN
eurjchem-1369	251	5	.	.	PUNCT
eurjchem-1369	252	1	yield	yield	NOUN
eurjchem-1369	252	2	:	:	PUNCT
eurjchem-1369	252	3	82	82	NUM
eurjchem-1369	252	4	%	%	NOUN
eurjchem-1369	252	5	.	.	PUNCT
eurjchem-1369	253	1	m.p	m.p	PROPN
eurjchem-1369	253	2	.	.	PROPN
eurjchem-1369	253	3	:	:	PUNCT
eurjchem-1369	254	1	312‐314	312‐314	NUM
eurjchem-1369	254	2	°	°	SYM
eurjchem-1369	254	3	c	c	X
eurjchem-1369	254	4	.	.	PUNCT
eurjchem-1369	255	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	255	2	(	(	PUNCT
eurjchem-1369	255	3	kbr	kbr	PROPN
eurjchem-1369	255	4	,	,	PUNCT
eurjchem-1369	255	5			PROPN
eurjchem-1369	255	6	,	,	PUNCT
eurjchem-1369	255	7	cm‐1	cm‐1	PROPN
eurjchem-1369	255	8	):	):	PUNCT
eurjchem-1369	255	9	3355‐3656	3355‐3656	NUM
eurjchem-1369	255	10	(	(	PUNCT
eurjchem-1369	255	11	nh2	nh2	PROPN
eurjchem-1369	255	12	)	)	PUNCT
eurjchem-1369	255	13	,	,	PUNCT
eurjchem-1369	255	14	3165	3165	NUM
eurjchem-1369	255	15	(	(	PUNCT
eurjchem-1369	255	16	nh	nh	NOUN
eurjchem-1369	255	17	)	)	PUNCT
eurjchem-1369	255	18	,	,	PUNCT
eurjchem-1369	255	19	1725	1725	NUM
eurjchem-1369	255	20	,	,	PUNCT
eurjchem-1369	255	21	1695	1695	NUM
eurjchem-1369	255	22	(	(	PUNCT
eurjchem-1369	255	23	c	c	X
eurjchem-1369	255	24	=	=	SYM
eurjchem-1369	255	25	o	o	NOUN
eurjchem-1369	255	26	's	's	PART
eurjchem-1369	255	27	)	)	PUNCT
eurjchem-1369	255	28	.	.	PUNCT
eurjchem-1369	256	1	1h	1h	NUM
eurjchem-1369	256	2	nmr	nmr	NOUN
eurjchem-1369	256	3	(	(	PUNCT
eurjchem-1369	256	4	250	250	NUM
eurjchem-1369	256	5	mhz	mhz	NOUN
eurjchem-1369	256	6	,	,	PUNCT
eurjchem-1369	256	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	256	8	,	,	PUNCT
eurjchem-1369	256	9	δ	δ	PROPN
eurjchem-1369	256	10	,	,	PUNCT
eurjchem-1369	256	11	ppm	ppm	NUM
eurjchem-1369	256	12	):	):	PUNCT
eurjchem-1369	256	13	1.18‐1.32	1.18‐1.32	NUM
eurjchem-1369	256	14	(	(	PUNCT
eurjchem-1369	256	15	t	t	PROPN
eurjchem-1369	256	16	,	,	PUNCT
eurjchem-1369	256	17	3h	3h	NUM
eurjchem-1369	256	18	,	,	PUNCT
eurjchem-1369	256	19	ch3	ch3	PROPN
eurjchem-1369	256	20	)	)	PUNCT
eurjchem-1369	256	21	,	,	PUNCT
eurjchem-1369	256	22	4.15‐4.37	4.15‐4.37	NUM
eurjchem-1369	256	23	(	(	PUNCT
eurjchem-1369	256	24	q	q	NOUN
eurjchem-1369	256	25	,	,	PUNCT
eurjchem-1369	256	26	2h	2h	NUM
eurjchem-1369	256	27	,	,	PUNCT
eurjchem-1369	256	28	ch2	ch2	PROPN
eurjchem-1369	256	29	)	)	PUNCT
eurjchem-1369	256	30	,	,	PUNCT
eurjchem-1369	256	31	6.95	6.95	NUM
eurjchem-1369	256	32	(	(	PUNCT
eurjchem-1369	256	33	br.s	br.s	PROPN
eurjchem-1369	256	34	,	,	PUNCT
eurjchem-1369	256	35	2h	2h	NUM
eurjchem-1369	256	36	,	,	PUNCT
eurjchem-1369	256	37	nh2	nh2	PROPN
eurjchem-1369	256	38	)	)	PUNCT
eurjchem-1369	256	39	,	,	PUNCT
eurjchem-1369	256	40	7.45‐8.15	7.45‐8.15	NUM
eurjchem-1369	256	41	(	(	PUNCT
eurjchem-1369	256	42	m	m	PROPN
eurjchem-1369	256	43	,	,	PUNCT
eurjchem-1369	256	44	4h	4h	NUM
eurjchem-1369	256	45	,	,	PUNCT
eurjchem-1369	256	46	ar'h	ar'h	NOUN
eurjchem-1369	256	47	)	)	PUNCT
eurjchem-1369	256	48	,	,	PUNCT
eurjchem-1369	256	49	8.30	8.30	NUM
eurjchem-1369	256	50	(	(	PUNCT
eurjchem-1369	256	51	s	s	PROPN
eurjchem-1369	256	52	,	,	PUNCT
eurjchem-1369	256	53	1h	1h	NUM
eurjchem-1369	256	54	,	,	PUNCT
eurjchem-1369	256	55	nh	nh	PROPN
eurjchem-1369	256	56	)	)	PUNCT
eurjchem-1369	256	57	,	,	PUNCT
eurjchem-1369	256	58	9.20	9.20	NUM
eurjchem-1369	256	59	(	(	PUNCT
eurjchem-1369	256	60	s	s	PROPN
eurjchem-1369	256	61	,	,	PUNCT
eurjchem-1369	256	62	1h	1h	NUM
eurjchem-1369	256	63	,	,	PUNCT
eurjchem-1369	256	64	ch‐	ch‐	NOUN
eurjchem-1369	256	65	quinazoline	quinazoline	NOUN
eurjchem-1369	256	66	)	)	PUNCT
eurjchem-1369	256	67	.	.	PUNCT
eurjchem-1369	257	1	ms	ms	NOUN
eurjchem-1369	257	2	(	(	PUNCT
eurjchem-1369	257	3	ei	ei	PROPN
eurjchem-1369	257	4	,	,	PUNCT
eurjchem-1369	257	5	m	m	PROPN
eurjchem-1369	257	6	/	/	SYM
eurjchem-1369	257	7	z	z	PROPN
eurjchem-1369	257	8	(	(	PUNCT
eurjchem-1369	257	9	%	%	NOUN
eurjchem-1369	257	10	)	)	PUNCT
eurjchem-1369	257	11	):	):	PUNCT
eurjchem-1369	257	12	299	299	NUM
eurjchem-1369	257	13	(	(	PUNCT
eurjchem-1369	257	14	m+	m+	NUM
eurjchem-1369	257	15	,	,	PUNCT
eurjchem-1369	257	16	18	18	NUM
eurjchem-1369	257	17	)	)	PUNCT
eurjchem-1369	257	18	.	.	PUNCT
eurjchem-1369	258	1	anal	anal	PROPN
eurjchem-1369	258	2	.	.	PUNCT
eurjchem-1369	258	3	calcd	calcd	NOUN
eurjchem-1369	258	4	.	.	PUNCT
eurjchem-1369	259	1	for	for	ADP
eurjchem-1369	259	2	c14h13n5o3	c14h13n5o3	PROPN
eurjchem-1369	259	3	:	:	PUNCT
eurjchem-1369	259	4	c	c	X
eurjchem-1369	259	5	,	,	PUNCT
eurjchem-1369	259	6	56.18	56.18	NUM
eurjchem-1369	259	7	;	;	PUNCT
eurjchem-1369	259	8	h	h	NOUN
eurjchem-1369	259	9	,	,	PUNCT
eurjchem-1369	259	10	4.38	4.38	NUM
eurjchem-1369	259	11	;	;	PUNCT
eurjchem-1369	259	12	n	n	CCONJ
eurjchem-1369	259	13	,	,	PUNCT
eurjchem-1369	259	14	23.40	23.40	NUM
eurjchem-1369	259	15	.	.	PUNCT
eurjchem-1369	259	16	found	find	VERB
eurjchem-1369	259	17	:	:	PUNCT
eurjchem-1369	260	1	c	c	X
eurjchem-1369	260	2	,	,	PUNCT
eurjchem-1369	260	3	56.45	56.45	NUM
eurjchem-1369	260	4	;	;	PUNCT
eurjchem-1369	261	1	h	h	NOUN
eurjchem-1369	261	2	,	,	PUNCT
eurjchem-1369	261	3	4.24	4.24	NUM
eurjchem-1369	261	4	;	;	PUNCT
eurjchem-1369	261	5	n	n	CCONJ
eurjchem-1369	261	6	,	,	PUNCT
eurjchem-1369	261	7	23.72	23.72	NUM
eurjchem-1369	261	8	%	%	NOUN
eurjchem-1369	261	9	.	.	PUNCT
eurjchem-1369	262	1	2.2.10	2.2.10	NUM
eurjchem-1369	262	2	.	.	PUNCT
eurjchem-1369	263	1	synthesis	synthesis	NOUN
eurjchem-1369	263	2	of	of	ADP
eurjchem-1369	263	3	diazotization	diazotization	NOUN
eurjchem-1369	263	4	of	of	ADP
eurjchem-1369	263	5	5‐amino‐3‐ureido‐1h‐	5‐amino‐3‐ureido‐1h‐	PROPN
eurjchem-1369	263	6	pyrazole‐4‐carboxylic	pyrazole‐4‐carboxylic	PROPN
eurjchem-1369	263	7	acid	acid	PROPN
eurjchem-1369	263	8	ethyl	ethyl	PROPN
eurjchem-1369	263	9	ester	ester	NOUN
eurjchem-1369	263	10	(	(	PUNCT
eurjchem-1369	263	11	4a	4a	NUM
eurjchem-1369	263	12	)	)	PUNCT
eurjchem-1369	263	13	a	a	DET
eurjchem-1369	263	14	cold	cold	ADJ
eurjchem-1369	263	15	solution	solution	NOUN
eurjchem-1369	263	16	of	of	ADP
eurjchem-1369	263	17	sodium	sodium	NOUN
eurjchem-1369	263	18	nitrite	nitrite	NOUN
eurjchem-1369	263	19	1.5	1.5	NUM
eurjchem-1369	263	20	g	g	NOUN
eurjchem-1369	263	21	in	in	ADP
eurjchem-1369	263	22	(	(	PUNCT
eurjchem-1369	263	23	10	10	NUM
eurjchem-1369	263	24	ml	ml	NOUN
eurjchem-1369	263	25	)	)	PUNCT
eurjchem-1369	263	26	of	of	ADP
eurjchem-1369	263	27	water	water	NOUN
eurjchem-1369	263	28	was	be	AUX
eurjchem-1369	263	29	added	add	VERB
eurjchem-1369	263	30	dropwisely	dropwisely	ADV
eurjchem-1369	263	31	to	to	ADP
eurjchem-1369	263	32	a	a	DET
eurjchem-1369	263	33	stirred	stirred	ADJ
eurjchem-1369	263	34	mixture	mixture	NOUN
eurjchem-1369	263	35	of	of	ADP
eurjchem-1369	263	36	compound	compound	NOUN
eurjchem-1369	263	37	4a	4a	NOUN
eurjchem-1369	263	38	(	(	PUNCT
eurjchem-1369	263	39	2.13	2.13	NUM
eurjchem-1369	263	40	g	g	NOUN
eurjchem-1369	263	41	,	,	PUNCT
eurjchem-1369	263	42	0.01	0.01	NUM
eurjchem-1369	263	43	mole	mole	NOUN
eurjchem-1369	263	44	)	)	PUNCT
eurjchem-1369	263	45	,	,	PUNCT
eurjchem-1369	263	46	hcl	hcl	PROPN
eurjchem-1369	263	47	(	(	PUNCT
eurjchem-1369	263	48	10	10	NUM
eurjchem-1369	263	49	ml	ml	NOUN
eurjchem-1369	263	50	,	,	PUNCT
eurjchem-1369	263	51	5	5	NUM
eurjchem-1369	263	52	%	%	NOUN
eurjchem-1369	263	53	)	)	PUNCT
eurjchem-1369	263	54	and	and	CCONJ
eurjchem-1369	263	55	glacial	glacial	ADJ
eurjchem-1369	263	56	acetic	acetic	ADJ
eurjchem-1369	263	57	acid	acid	NOUN
eurjchem-1369	263	58	(	(	PUNCT
eurjchem-1369	263	59	10	10	NUM
eurjchem-1369	263	60	ml	ml	NOUN
eurjchem-1369	263	61	)	)	PUNCT
eurjchem-1369	263	62	.	.	PUNCT
eurjchem-1369	264	1	the	the	DET
eurjchem-1369	264	2	mixture	mixture	NOUN
eurjchem-1369	264	3	was	be	AUX
eurjchem-1369	264	4	stirred	stir	VERB
eurjchem-1369	264	5	at	at	ADP
eurjchem-1369	264	6	0‐5	0‐5	NOUN
eurjchem-1369	264	7	°	°	ADP
eurjchem-1369	264	8	c	c	NOUN
eurjchem-1369	264	9	for	for	ADP
eurjchem-1369	264	10	1/2	1/2	NUM
eurjchem-1369	264	11	h	h	NOUN
eurjchem-1369	264	12	and	and	CCONJ
eurjchem-1369	264	13	the	the	DET
eurjchem-1369	264	14	resulting	result	VERB
eurjchem-1369	264	15	diazotized	diazotize	VERB
eurjchem-1369	264	16	solution	solution	NOUN
eurjchem-1369	264	17	17	17	NUM
eurjchem-1369	264	18	was	be	AUX
eurjchem-1369	264	19	used	use	VERB
eurjchem-1369	264	20	directly	directly	ADV
eurjchem-1369	264	21	in	in	ADP
eurjchem-1369	264	22	the	the	DET
eurjchem-1369	264	23	next	next	ADJ
eurjchem-1369	264	24	reactions	reaction	NOUN
eurjchem-1369	264	25	(	(	PUNCT
eurjchem-1369	264	26	scheme	scheme	NOUN
eurjchem-1369	264	27	5	5	NUM
eurjchem-1369	264	28	)	)	PUNCT
eurjchem-1369	264	29	.	.	PUNCT
eurjchem-1369	265	1	2.2.11	2.2.11	NUM
eurjchem-1369	265	2	.	.	PUNCT
eurjchem-1369	265	3	general	general	ADJ
eurjchem-1369	265	4	procedure	procedure	NOUN
eurjchem-1369	265	5	for	for	ADP
eurjchem-1369	265	6	coupling	coupling	NOUN
eurjchem-1369	265	7	of	of	ADP
eurjchem-1369	265	8	diazotized	diazotize	VERB
eurjchem-1369	265	9	17	17	NUM
eurjchem-1369	265	10	with	with	ADP
eurjchem-1369	265	11	2‐naphthol	2‐naphthol	NUM
eurjchem-1369	265	12	,	,	PUNCT
eurjchem-1369	265	13	resorcinol	resorcinol	NOUN
eurjchem-1369	265	14	,	,	PUNCT
eurjchem-1369	265	15	malononitrile	malononitrile	NOUN
eurjchem-1369	265	16	and	and	CCONJ
eurjchem-1369	265	17	ethylcyanoacetate	ethylcyanoacetate	VERB
eurjchem-1369	265	18	a	a	DET
eurjchem-1369	265	19	solution	solution	NOUN
eurjchem-1369	265	20	of	of	ADP
eurjchem-1369	265	21	diazonium	diazonium	NOUN
eurjchem-1369	265	22	salt	salt	NOUN
eurjchem-1369	265	23	17	17	NUM
eurjchem-1369	265	24	(	(	PUNCT
eurjchem-1369	265	25	0.01	0.01	NUM
eurjchem-1369	265	26	mole	mole	NOUN
eurjchem-1369	265	27	)	)	PUNCT
eurjchem-1369	265	28	was	be	AUX
eurjchem-1369	265	29	added	add	VERB
eurjchem-1369	265	30	to	to	ADP
eurjchem-1369	265	31	a	a	DET
eurjchem-1369	265	32	solution	solution	NOUN
eurjchem-1369	265	33	of	of	ADP
eurjchem-1369	265	34	the	the	DET
eurjchem-1369	265	35	appropriate	appropriate	ADJ
eurjchem-1369	265	36	coupling	coupling	NOUN
eurjchem-1369	265	37	reagent	reagent	NOUN
eurjchem-1369	265	38	namely	namely	ADV
eurjchem-1369	265	39	,	,	PUNCT
eurjchem-1369	265	40	2‐	2‐	NUM
eurjchem-1369	265	41	napthol	napthol	NOUN
eurjchem-1369	265	42	,	,	PUNCT
eurjchem-1369	265	43	resorcinol	resorcinol	NOUN
eurjchem-1369	265	44	,	,	PUNCT
eurjchem-1369	265	45	ethylcyanoacetate	ethylcyanoacetate	ADJ
eurjchem-1369	265	46	or	or	CCONJ
eurjchem-1369	265	47	malononitrile	malononitrile	NOUN
eurjchem-1369	265	48	(	(	PUNCT
eurjchem-1369	265	49	0.01	0.01	NUM
eurjchem-1369	265	50	mole	mole	NOUN
eurjchem-1369	265	51	)	)	PUNCT
eurjchem-1369	265	52	in	in	ADP
eurjchem-1369	265	53	ethanol	ethanol	NOUN
eurjchem-1369	265	54	(	(	PUNCT
eurjchem-1369	265	55	50	50	NUM
eurjchem-1369	265	56	ml	ml	NOUN
eurjchem-1369	265	57	)	)	PUNCT
eurjchem-1369	265	58	in	in	ADP
eurjchem-1369	265	59	the	the	DET
eurjchem-1369	265	60	presence	presence	NOUN
eurjchem-1369	265	61	of	of	ADP
eurjchem-1369	265	62	sodium	sodium	NOUN
eurjchem-1369	265	63	acetate	acetate	NOUN
eurjchem-1369	265	64	(	(	PUNCT
eurjchem-1369	265	65	5	5	NUM
eurjchem-1369	265	66	g	g	NOUN
eurjchem-1369	265	67	)	)	PUNCT
eurjchem-1369	265	68	.	.	PUNCT
eurjchem-1369	266	1	the	the	DET
eurjchem-1369	266	2	solid	solid	ADJ
eurjchem-1369	266	3	product	product	NOUN
eurjchem-1369	266	4	formed	form	VERB
eurjchem-1369	266	5	on	on	ADP
eurjchem-1369	266	6	standing	standing	NOUN
eurjchem-1369	266	7	was	be	AUX
eurjchem-1369	266	8	collected	collect	VERB
eurjchem-1369	266	9	by	by	ADP
eurjchem-1369	266	10	filtration	filtration	NOUN
eurjchem-1369	266	11	and	and	CCONJ
eurjchem-1369	266	12	crystallized	crystallize	VERB
eurjchem-1369	266	13	from	from	ADP
eurjchem-1369	266	14	the	the	DET
eurjchem-1369	266	15	appropriate	appropriate	ADJ
eurjchem-1369	266	16	solvent	solvent	NOUN
eurjchem-1369	266	17	to	to	PART
eurjchem-1369	266	18	give	give	VERB
eurjchem-1369	266	19	compound	compound	NOUN
eurjchem-1369	266	20	18	18	NUM
eurjchem-1369	266	21	,	,	PUNCT
eurjchem-1369	266	22	20	20	NUM
eurjchem-1369	266	23	,	,	PUNCT
eurjchem-1369	266	24	22a	22a	NUM
eurjchem-1369	266	25	and	and	CCONJ
eurjchem-1369	266	26	22b	22b	NOUN
eurjchem-1369	266	27	,	,	PUNCT
eurjchem-1369	266	28	respectively	respectively	ADV
eurjchem-1369	266	29	(	(	PUNCT
eurjchem-1369	266	30	scheme	scheme	NOUN
eurjchem-1369	266	31	5	5	NUM
eurjchem-1369	266	32	)	)	PUNCT
eurjchem-1369	266	33	.	.	PUNCT
eurjchem-1369	267	1	5‐(2‐hydroxy‐naphthalen‐1‐ylazo)‐3‐ureido‐1h‐pyrazole‐4‐	5‐(2‐hydroxy‐naphthalen‐1‐ylazo)‐3‐ureido‐1h‐pyrazole‐4‐	NUM
eurjchem-1369	267	2	carboxylic	carboxylic	ADJ
eurjchem-1369	267	3	acid	acid	NOUN
eurjchem-1369	267	4	ethyl	ethyl	PROPN
eurjchem-1369	267	5	ester	ester	NOUN
eurjchem-1369	267	6	(	(	PUNCT
eurjchem-1369	267	7	18	18	NUM
eurjchem-1369	267	8	):	):	PUNCT
eurjchem-1369	267	9	color	color	NOUN
eurjchem-1369	267	10	:	:	PUNCT
eurjchem-1369	267	11	red	red	ADJ
eurjchem-1369	267	12	crystals	crystal	NOUN
eurjchem-1369	267	13	.	.	PUNCT
eurjchem-1369	268	1	yield	yield	NOUN
eurjchem-1369	268	2	:	:	PUNCT
eurjchem-1369	268	3	65	65	NUM
eurjchem-1369	268	4	%	%	NOUN
eurjchem-1369	268	5	.	.	PUNCT
eurjchem-1369	269	1	m.p	m.p	PROPN
eurjchem-1369	269	2	.	.	PROPN
eurjchem-1369	269	3	:	:	PUNCT
eurjchem-1369	270	1	312‐314	312‐314	NUM
eurjchem-1369	270	2	°	°	SYM
eurjchem-1369	270	3	c	c	X
eurjchem-1369	270	4	.	.	PUNCT
eurjchem-1369	271	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	271	2	(	(	PUNCT
eurjchem-1369	271	3	kbr	kbr	PROPN
eurjchem-1369	271	4	,	,	PUNCT
eurjchem-1369	271	5			PROPN
eurjchem-1369	271	6	,	,	PUNCT
eurjchem-1369	271	7	cm‐1	cm‐1	PROPN
eurjchem-1369	271	8	):	):	PUNCT
eurjchem-1369	271	9	3445‐3326	3445‐3326	NUM
eurjchem-1369	271	10	(	(	PUNCT
eurjchem-1369	271	11	nh2	nh2	NOUN
eurjchem-1369	271	12	and	and	CCONJ
eurjchem-1369	271	13	oh	oh	INTJ
eurjchem-1369	271	14	)	)	PUNCT
eurjchem-1369	271	15	,	,	PUNCT
eurjchem-1369	271	16	3165	3165	NUM
eurjchem-1369	271	17	(	(	PUNCT
eurjchem-1369	271	18	nh	nh	NOUN
eurjchem-1369	271	19	)	)	PUNCT
eurjchem-1369	271	20	,	,	PUNCT
eurjchem-1369	271	21	1720	1720	NUM
eurjchem-1369	271	22	,	,	PUNCT
eurjchem-1369	271	23	1682	1682	NUM
eurjchem-1369	271	24	(	(	PUNCT
eurjchem-1369	271	25	c	c	X
eurjchem-1369	271	26	=	=	SYM
eurjchem-1369	271	27	o	o	NOUN
eurjchem-1369	271	28	's	's	PART
eurjchem-1369	271	29	)	)	PUNCT
eurjchem-1369	271	30	.	.	PUNCT
eurjchem-1369	272	1	1h	1h	NUM
eurjchem-1369	272	2	nmr	nmr	NOUN
eurjchem-1369	272	3	(	(	PUNCT
eurjchem-1369	272	4	250	250	NUM
eurjchem-1369	272	5	mhz	mhz	NOUN
eurjchem-1369	272	6	,	,	PUNCT
eurjchem-1369	272	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	272	8	,	,	PUNCT
eurjchem-1369	272	9	δ	δ	PROPN
eurjchem-1369	272	10	,	,	PUNCT
eurjchem-1369	272	11	ppm	ppm	NUM
eurjchem-1369	272	12	):	):	PUNCT
eurjchem-1369	272	13	1.22‐1.32	1.22‐1.32	NUM
eurjchem-1369	272	14	(	(	PUNCT
eurjchem-1369	272	15	t	t	PROPN
eurjchem-1369	272	16	,	,	PUNCT
eurjchem-1369	272	17	3h	3h	NUM
eurjchem-1369	272	18	,	,	PUNCT
eurjchem-1369	272	19	ch3	ch3	PROPN
eurjchem-1369	272	20	)	)	PUNCT
eurjchem-1369	272	21	,	,	PUNCT
eurjchem-1369	272	22	3.62	3.62	NUM
eurjchem-1369	272	23	(	(	PUNCT
eurjchem-1369	272	24	s	s	PROPN
eurjchem-1369	272	25	,	,	PUNCT
eurjchem-1369	272	26	1h	1h	NUM
eurjchem-1369	272	27	,	,	PUNCT
eurjchem-1369	272	28	pyrazole‐	pyrazole‐	NOUN
eurjchem-1369	272	29	h	h	NOUN
eurjchem-1369	272	30	)	)	PUNCT
eurjchem-1369	272	31	,	,	PUNCT
eurjchem-1369	272	32	4.15‐4.27	4.15‐4.27	NUM
eurjchem-1369	272	33	(	(	PUNCT
eurjchem-1369	272	34	q	q	NOUN
eurjchem-1369	272	35	,	,	PUNCT
eurjchem-1369	272	36	2h	2h	NUM
eurjchem-1369	272	37	,	,	PUNCT
eurjchem-1369	272	38	ch2	ch2	PROPN
eurjchem-1369	272	39	)	)	PUNCT
eurjchem-1369	272	40	,	,	PUNCT
eurjchem-1369	272	41	6.60	6.60	NUM
eurjchem-1369	272	42	(	(	PUNCT
eurjchem-1369	272	43	s	s	NOUN
eurjchem-1369	272	44	,	,	PUNCT
eurjchem-1369	272	45	2h	2h	NUM
eurjchem-1369	272	46	,	,	PUNCT
eurjchem-1369	272	47	nh2	nh2	PROPN
eurjchem-1369	272	48	)	)	PUNCT
eurjchem-1369	272	49	,	,	PUNCT
eurjchem-1369	272	50	7.25‐8.90	7.25‐8.90	NUM
eurjchem-1369	272	51	(	(	PUNCT
eurjchem-1369	272	52	m	m	PROPN
eurjchem-1369	272	53	,	,	PUNCT
eurjchem-1369	272	54	6h	6h	NUM
eurjchem-1369	272	55	,	,	PUNCT
eurjchem-1369	272	56	ar'h	ar'h	NOUN
eurjchem-1369	272	57	)	)	PUNCT
eurjchem-1369	272	58	,	,	PUNCT
eurjchem-1369	272	59	10.80	10.80	NUM
eurjchem-1369	272	60	(	(	PUNCT
eurjchem-1369	272	61	br.s	br.s	PROPN
eurjchem-1369	272	62	,	,	PUNCT
eurjchem-1369	272	63	1h	1h	NUM
eurjchem-1369	272	64	,	,	PUNCT
eurjchem-1369	272	65	oh	oh	INTJ
eurjchem-1369	272	66	)	)	PUNCT
eurjchem-1369	272	67	,	,	PUNCT
eurjchem-1369	272	68	12.15	12.15	NUM
eurjchem-1369	272	69	(	(	PUNCT
eurjchem-1369	272	70	s	s	PROPN
eurjchem-1369	272	71	,	,	PUNCT
eurjchem-1369	272	72	1h	1h	NUM
eurjchem-1369	272	73	,	,	PUNCT
eurjchem-1369	272	74	nh	nh	PROPN
eurjchem-1369	272	75	)	)	PUNCT
eurjchem-1369	272	76	.	.	PUNCT
eurjchem-1369	273	1	ms	ms	NOUN
eurjchem-1369	273	2	(	(	PUNCT
eurjchem-1369	273	3	ei	ei	PROPN
eurjchem-1369	273	4	,	,	PUNCT
eurjchem-1369	273	5	m	m	PROPN
eurjchem-1369	273	6	/	/	SYM
eurjchem-1369	273	7	z	z	PROPN
eurjchem-1369	273	8	(	(	PUNCT
eurjchem-1369	273	9	%	%	NOUN
eurjchem-1369	273	10	)	)	PUNCT
eurjchem-1369	273	11	):	):	PUNCT
eurjchem-1369	273	12	368	368	NUM
eurjchem-1369	273	13	(	(	PUNCT
eurjchem-1369	273	14	m+	m+	NUM
eurjchem-1369	273	15	,	,	PUNCT
eurjchem-1369	273	16	26	26	NUM
eurjchem-1369	273	17	)	)	PUNCT
eurjchem-1369	273	18	.	.	PUNCT
eurjchem-1369	274	1	anal	anal	PROPN
eurjchem-1369	274	2	.	.	PUNCT
eurjchem-1369	274	3	calcd	calcd	NOUN
eurjchem-1369	274	4	.	.	PUNCT
eurjchem-1369	275	1	for	for	ADP
eurjchem-1369	275	2	c17h16n6o4	c17h16n6o4	PROPN
eurjchem-1369	275	3	:	:	PUNCT
eurjchem-1369	275	4	c	c	X
eurjchem-1369	275	5	,	,	PUNCT
eurjchem-1369	275	6	55.43	55.43	NUM
eurjchem-1369	275	7	;	;	PUNCT
eurjchem-1369	275	8	h	h	NOUN
eurjchem-1369	275	9	,	,	PUNCT
eurjchem-1369	275	10	4.38	4.38	NUM
eurjchem-1369	275	11	;	;	PUNCT
eurjchem-1369	275	12	n	n	CCONJ
eurjchem-1369	275	13	,	,	PUNCT
eurjchem-1369	275	14	22.82	22.82	NUM
eurjchem-1369	275	15	.	.	PUNCT
eurjchem-1369	275	16	found	find	VERB
eurjchem-1369	275	17	:	:	PUNCT
eurjchem-1369	276	1	c	c	X
eurjchem-1369	276	2	,	,	PUNCT
eurjchem-1369	276	3	55.66	55.66	NUM
eurjchem-1369	276	4	;	;	PUNCT
eurjchem-1369	276	5	h	h	X
eurjchem-1369	276	6	,	,	PUNCT
eurjchem-1369	276	7	4.63	4.63	NUM
eurjchem-1369	276	8	;	;	PUNCT
eurjchem-1369	276	9	n	n	CCONJ
eurjchem-1369	276	10	,	,	PUNCT
eurjchem-1369	276	11	22.71	22.71	NUM
eurjchem-1369	276	12	%	%	NOUN
eurjchem-1369	276	13	.	.	PUNCT
eurjchem-1369	277	1	5‐(2,4‐dihydroxy‐phenylazo)‐3‐ureido‐1h‐pyrazole‐4‐carbo‐	5‐(2,4‐dihydroxy‐phenylazo)‐3‐ureido‐1h‐pyrazole‐4‐carbo‐	NUM
eurjchem-1369	277	2	xylic	xylic	PROPN
eurjchem-1369	277	3	acid	acid	PROPN
eurjchem-1369	277	4	ethyl	ethyl	PROPN
eurjchem-1369	277	5	ester	ester	NOUN
eurjchem-1369	277	6	(	(	PUNCT
eurjchem-1369	277	7	20	20	NUM
eurjchem-1369	277	8	):	):	PUNCT
eurjchem-1369	277	9	color	color	NOUN
eurjchem-1369	277	10	:	:	PUNCT
eurjchem-1369	277	11	orange	orange	ADJ
eurjchem-1369	277	12	crystals	crystal	NOUN
eurjchem-1369	277	13	.	.	PUNCT
eurjchem-1369	278	1	yield	yield	NOUN
eurjchem-1369	278	2	:	:	PUNCT
eurjchem-1369	278	3	83	83	NUM
eurjchem-1369	278	4	%	%	NOUN
eurjchem-1369	278	5	.	.	PUNCT
eurjchem-1369	279	1	m.p	m.p	PROPN
eurjchem-1369	279	2	.	.	PROPN
eurjchem-1369	279	3	:	:	PUNCT
eurjchem-1369	280	1	337‐339	337‐339	PROPN
eurjchem-1369	280	2	°	°	SYM
eurjchem-1369	280	3	c	c	PROPN
eurjchem-1369	280	4	.	.	PUNCT
eurjchem-1369	281	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	281	2	(	(	PUNCT
eurjchem-1369	281	3	kbr	kbr	PROPN
eurjchem-1369	281	4	,	,	PUNCT
eurjchem-1369	281	5			PROPN
eurjchem-1369	281	6	,	,	PUNCT
eurjchem-1369	281	7	cm‐1	cm‐1	PROPN
eurjchem-1369	281	8	):	):	PUNCT
eurjchem-1369	281	9	3445‐3315	3445‐3315	PROPN
eurjchem-1369	281	10	(	(	PUNCT
eurjchem-1369	281	11	nh2	nh2	PROPN
eurjchem-1369	281	12	and	and	CCONJ
eurjchem-1369	281	13	oh	oh	INTJ
eurjchem-1369	281	14	)	)	PUNCT
eurjchem-1369	281	15	,	,	PUNCT
eurjchem-1369	281	16	3165	3165	NUM
eurjchem-1369	281	17	(	(	PUNCT
eurjchem-1369	281	18	nh	nh	NOUN
eurjchem-1369	281	19	)	)	PUNCT
eurjchem-1369	281	20	,	,	PUNCT
eurjchem-1369	281	21	1720	1720	NUM
eurjchem-1369	281	22	,	,	PUNCT
eurjchem-1369	281	23	1682	1682	NUM
eurjchem-1369	281	24	(	(	PUNCT
eurjchem-1369	281	25	c	c	X
eurjchem-1369	281	26	=	=	SYM
eurjchem-1369	281	27	o	o	NOUN
eurjchem-1369	281	28	's	's	PART
eurjchem-1369	281	29	)	)	PUNCT
eurjchem-1369	281	30	.	.	PUNCT
eurjchem-1369	282	1	1h	1h	NUM
eurjchem-1369	282	2	nmr	nmr	NOUN
eurjchem-1369	282	3	(	(	PUNCT
eurjchem-1369	282	4	250	250	NUM
eurjchem-1369	282	5	mhz	mhz	NOUN
eurjchem-1369	282	6	,	,	PUNCT
eurjchem-1369	282	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	282	8	,	,	PUNCT
eurjchem-1369	282	9	δ	δ	PROPN
eurjchem-1369	282	10	,	,	PUNCT
eurjchem-1369	282	11	ppm	ppm	NUM
eurjchem-1369	282	12	):	):	PUNCT
eurjchem-1369	282	13	1.18‐1.37	1.18‐1.37	NUM
eurjchem-1369	282	14	(	(	PUNCT
eurjchem-1369	282	15	t	t	PROPN
eurjchem-1369	282	16	,	,	PUNCT
eurjchem-1369	282	17	3h	3h	NUM
eurjchem-1369	282	18	,	,	PUNCT
eurjchem-1369	282	19	ch3	ch3	PROPN
eurjchem-1369	282	20	)	)	PUNCT
eurjchem-1369	282	21	,	,	PUNCT
eurjchem-1369	282	22	3.69	3.69	NUM
eurjchem-1369	282	23	(	(	PUNCT
eurjchem-1369	282	24	s	s	PROPN
eurjchem-1369	282	25	,	,	PUNCT
eurjchem-1369	282	26	1h	1h	NUM
eurjchem-1369	282	27	,	,	PUNCT
eurjchem-1369	282	28	pyrazole‐	pyrazole‐	NOUN
eurjchem-1369	282	29	h	h	NOUN
eurjchem-1369	282	30	)	)	PUNCT
eurjchem-1369	282	31	,	,	PUNCT
eurjchem-1369	282	32	4.16‐4.28	4.16‐4.28	PROPN
eurjchem-1369	282	33	(	(	PUNCT
eurjchem-1369	282	34	q	q	NOUN
eurjchem-1369	282	35	,	,	PUNCT
eurjchem-1369	282	36	2h	2h	NUM
eurjchem-1369	282	37	,	,	PUNCT
eurjchem-1369	282	38	ch2	ch2	PROPN
eurjchem-1369	282	39	)	)	PUNCT
eurjchem-1369	282	40	,	,	PUNCT
eurjchem-1369	282	41	6.62	6.62	NUM
eurjchem-1369	282	42	(	(	PUNCT
eurjchem-1369	282	43	br.s	br.s	PROPN
eurjchem-1369	282	44	,	,	PUNCT
eurjchem-1369	282	45	2h	2h	NUM
eurjchem-1369	282	46	,	,	PUNCT
eurjchem-1369	282	47	nh2	nh2	PROPN
eurjchem-1369	282	48	)	)	PUNCT
eurjchem-1369	282	49	,	,	PUNCT
eurjchem-1369	282	50	7.26‐8.12	7.26‐8.12	NUM
eurjchem-1369	282	51	(	(	PUNCT
eurjchem-1369	282	52	m	m	PROPN
eurjchem-1369	282	53	,	,	PUNCT
eurjchem-1369	282	54	3h	3h	NUM
eurjchem-1369	282	55	,	,	PUNCT
eurjchem-1369	282	56	ar‐h	ar‐h	NOUN
eurjchem-1369	282	57	)	)	PUNCT
eurjchem-1369	282	58	,	,	PUNCT
eurjchem-1369	282	59	11.2	11.2	NUM
eurjchem-1369	282	60	(	(	PUNCT
eurjchem-1369	282	61	s	s	PROPN
eurjchem-1369	282	62	,	,	PUNCT
eurjchem-1369	282	63	1h	1h	NUM
eurjchem-1369	282	64	,	,	PUNCT
eurjchem-1369	282	65	nh	nh	PROPN
eurjchem-1369	282	66	)	)	PUNCT
eurjchem-1369	282	67	,	,	PUNCT
eurjchem-1369	282	68	12.15	12.15	NUM
eurjchem-1369	282	69	(	(	PUNCT
eurjchem-1369	282	70	br.s	br.s	PROPN
eurjchem-1369	282	71	,	,	PUNCT
eurjchem-1369	282	72	2h	2h	NUM
eurjchem-1369	282	73	,	,	PUNCT
eurjchem-1369	282	74	2oh	2oh	NOUN
eurjchem-1369	282	75	)	)	PUNCT
eurjchem-1369	282	76	.	.	PUNCT
eurjchem-1369	283	1	ms	ms	NOUN
eurjchem-1369	283	2	(	(	PUNCT
eurjchem-1369	283	3	ei	ei	PROPN
eurjchem-1369	283	4	,	,	PUNCT
eurjchem-1369	283	5	m	m	PROPN
eurjchem-1369	283	6	/	/	SYM
eurjchem-1369	283	7	z	z	PROPN
eurjchem-1369	283	8	(	(	PUNCT
eurjchem-1369	283	9	%	%	NOUN
eurjchem-1369	283	10	)	)	PUNCT
eurjchem-1369	283	11	):	):	PUNCT
eurjchem-1369	283	12	334	334	NUM
eurjchem-1369	283	13	(	(	PUNCT
eurjchem-1369	283	14	m+	m+	NUM
eurjchem-1369	283	15	,	,	PUNCT
eurjchem-1369	283	16	34	34	NUM
eurjchem-1369	283	17	)	)	PUNCT
eurjchem-1369	283	18	.	.	PUNCT
eurjchem-1369	284	1	anal	anal	PROPN
eurjchem-1369	284	2	.	.	PUNCT
eurjchem-1369	284	3	calcd	calcd	NOUN
eurjchem-1369	284	4	.	.	PUNCT
eurjchem-1369	285	1	for	for	ADP
eurjchem-1369	285	2	c13h14n6o5	c13h14n6o5	PROPN
eurjchem-1369	285	3	:	:	PUNCT
eurjchem-1369	285	4	c	c	X
eurjchem-1369	285	5	,	,	PUNCT
eurjchem-1369	285	6	46.71	46.71	NUM
eurjchem-1369	285	7	;	;	PUNCT
eurjchem-1369	285	8	h	h	NOUN
eurjchem-1369	285	9	,	,	PUNCT
eurjchem-1369	285	10	4.22	4.22	NUM
eurjchem-1369	285	11	;	;	PUNCT
eurjchem-1369	285	12	n	n	CCONJ
eurjchem-1369	285	13	,	,	PUNCT
eurjchem-1369	285	14	25.14	25.14	NUM
eurjchem-1369	285	15	.	.	PUNCT
eurjchem-1369	286	1	found	find	VERB
eurjchem-1369	286	2	:	:	PUNCT
eurjchem-1369	287	1	c	c	X
eurjchem-1369	287	2	,	,	PUNCT
eurjchem-1369	287	3	46.53	46.53	NUM
eurjchem-1369	287	4	;	;	PUNCT
eurjchem-1369	287	5	h	h	NOUN
eurjchem-1369	287	6	,	,	PUNCT
eurjchem-1369	287	7	4.33	4.33	NUM
eurjchem-1369	287	8	;	;	PUNCT
eurjchem-1369	287	9	n	n	CCONJ
eurjchem-1369	287	10	,	,	PUNCT
eurjchem-1369	287	11	25.43	25.43	NUM
eurjchem-1369	287	12	%	%	NOUN
eurjchem-1369	287	13	.	.	PUNCT
eurjchem-1369	288	1	4‐amino‐7‐ureido‐pyrazolo[5,1‐c][1,2,4]triazine‐3,8‐di	4‐amino‐7‐ureido‐pyrazolo[5,1‐c][1,2,4]triazine‐3,8‐di	NUM
eurjchem-1369	288	2	carbo‐	carbo‐	VERB
eurjchem-1369	288	3	xylic	xylic	PROPN
eurjchem-1369	288	4	acid	acid	PROPN
eurjchem-1369	288	5	diethyl	diethyl	NOUN
eurjchem-1369	288	6	ester	ester	NOUN
eurjchem-1369	288	7	(	(	PUNCT
eurjchem-1369	288	8	22a	22a	NUM
eurjchem-1369	288	9	):	):	PUNCT
eurjchem-1369	288	10	color	color	NOUN
eurjchem-1369	288	11	:	:	PUNCT
eurjchem-1369	288	12	yellow	yellow	ADJ
eurjchem-1369	288	13	crystals	crystal	NOUN
eurjchem-1369	288	14	.	.	PUNCT
eurjchem-1369	289	1	yield	yield	NOUN
eurjchem-1369	289	2	:	:	PUNCT
eurjchem-1369	289	3	74	74	NUM
eurjchem-1369	289	4	%	%	NOUN
eurjchem-1369	289	5	.	.	PUNCT
eurjchem-1369	290	1	m.p	m.p	PROPN
eurjchem-1369	290	2	.	.	PROPN
eurjchem-1369	290	3	:	:	PUNCT
eurjchem-1369	291	1	341‐343	341‐343	PROPN
eurjchem-1369	291	2	°	°	SYM
eurjchem-1369	291	3	c	c	PROPN
eurjchem-1369	291	4	.	.	PUNCT
eurjchem-1369	292	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	292	2	(	(	PUNCT
eurjchem-1369	292	3	kbr	kbr	PROPN
eurjchem-1369	292	4	,	,	PUNCT
eurjchem-1369	292	5			PROPN
eurjchem-1369	292	6	,	,	PUNCT
eurjchem-1369	292	7	cm‐1	cm‐1	PROPN
eurjchem-1369	292	8	):	):	PUNCT
eurjchem-1369	292	9	3345‐3326	3345‐3326	NUM
eurjchem-1369	292	10	(	(	PUNCT
eurjchem-1369	292	11	nh2	nh2	PROPN
eurjchem-1369	292	12	)	)	PUNCT
eurjchem-1369	292	13	,	,	PUNCT
eurjchem-1369	292	14	3165	3165	NUM
eurjchem-1369	292	15	(	(	PUNCT
eurjchem-1369	292	16	nh	nh	NOUN
eurjchem-1369	292	17	)	)	PUNCT
eurjchem-1369	292	18	,	,	PUNCT
eurjchem-1369	292	19	1720	1720	NUM
eurjchem-1369	292	20	,	,	PUNCT
eurjchem-1369	292	21	1682	1682	NUM
eurjchem-1369	292	22	(	(	PUNCT
eurjchem-1369	292	23	c	c	X
eurjchem-1369	292	24	=	=	SYM
eurjchem-1369	292	25	o	o	NOUN
eurjchem-1369	292	26	's	's	PART
eurjchem-1369	292	27	)	)	PUNCT
eurjchem-1369	292	28	.	.	PUNCT
eurjchem-1369	293	1	1h	1h	NUM
eurjchem-1369	293	2	nmr	nmr	NOUN
eurjchem-1369	293	3	(	(	PUNCT
eurjchem-1369	293	4	250	250	NUM
eurjchem-1369	293	5	mhz	mhz	NOUN
eurjchem-1369	293	6	,	,	PUNCT
eurjchem-1369	293	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	293	8	,	,	PUNCT
eurjchem-1369	293	9	δ	δ	PROPN
eurjchem-1369	293	10	,	,	PUNCT
eurjchem-1369	293	11	ppm	ppm	NUM
eurjchem-1369	293	12	):	):	PUNCT
eurjchem-1369	293	13	1.15‐1.38	1.15‐1.38	NUM
eurjchem-1369	293	14	(	(	PUNCT
eurjchem-1369	293	15	m	m	PROPN
eurjchem-1369	293	16	,	,	PUNCT
eurjchem-1369	293	17	6h	6h	NUM
eurjchem-1369	293	18	,	,	PUNCT
eurjchem-1369	293	19	2ch3	2ch3	NUM
eurjchem-1369	293	20	)	)	PUNCT
eurjchem-1369	293	21	,	,	PUNCT
eurjchem-1369	293	22	4.33‐4.35	4.33‐4.35	NUM
eurjchem-1369	293	23	(	(	PUNCT
eurjchem-1369	293	24	m	m	PROPN
eurjchem-1369	293	25	,	,	PUNCT
eurjchem-1369	293	26	4h	4h	NOUN
eurjchem-1369	293	27	,	,	PUNCT
eurjchem-1369	293	28	2ch2	2ch2	NUM
eurjchem-1369	293	29	)	)	PUNCT
eurjchem-1369	293	30	,	,	PUNCT
eurjchem-1369	293	31	6.67	6.67	NUM
eurjchem-1369	293	32	(	(	PUNCT
eurjchem-1369	293	33	s	s	PROPN
eurjchem-1369	293	34	,	,	PUNCT
eurjchem-1369	293	35	2h	2h	NUM
eurjchem-1369	293	36	,	,	PUNCT
eurjchem-1369	293	37	nh2	nh2	PROPN
eurjchem-1369	293	38	)	)	PUNCT
eurjchem-1369	293	39	,	,	PUNCT
eurjchem-1369	293	40	7.2	7.2	NUM
eurjchem-1369	293	41	(	(	PUNCT
eurjchem-1369	293	42	br.s	br.s	PROPN
eurjchem-1369	293	43	,	,	PUNCT
eurjchem-1369	293	44	2h	2h	NUM
eurjchem-1369	293	45	,	,	PUNCT
eurjchem-1369	293	46	nh2	nh2	PROPN
eurjchem-1369	293	47	)	)	PUNCT
eurjchem-1369	293	48	,	,	PUNCT
eurjchem-1369	293	49	8.4	8.4	NUM
eurjchem-1369	293	50	(	(	PUNCT
eurjchem-1369	293	51	s	s	PROPN
eurjchem-1369	293	52	,	,	PUNCT
eurjchem-1369	293	53	1h	1h	NUM
eurjchem-1369	293	54	,	,	PUNCT
eurjchem-1369	293	55	nh	nh	PROPN
eurjchem-1369	293	56	)	)	PUNCT
eurjchem-1369	293	57	.	.	PUNCT
eurjchem-1369	294	1	ms	ms	NOUN
eurjchem-1369	294	2	(	(	PUNCT
eurjchem-1369	294	3	ei	ei	PROPN
eurjchem-1369	294	4	,	,	PUNCT
eurjchem-1369	294	5	m	m	PROPN
eurjchem-1369	294	6	/	/	SYM
eurjchem-1369	294	7	z	z	PROPN
eurjchem-1369	294	8	(	(	PUNCT
eurjchem-1369	294	9	%	%	NOUN
eurjchem-1369	294	10	)	)	PUNCT
eurjchem-1369	294	11	):	):	PUNCT
eurjchem-1369	294	12	337	337	NUM
eurjchem-1369	294	13	(	(	PUNCT
eurjchem-1369	294	14	m+	m+	NUM
eurjchem-1369	294	15	,	,	PUNCT
eurjchem-1369	294	16	17	17	NUM
eurjchem-1369	294	17	)	)	PUNCT
eurjchem-1369	294	18	.	.	PUNCT
eurjchem-1369	295	1	anal	anal	PROPN
eurjchem-1369	295	2	.	.	PUNCT
eurjchem-1369	295	3	calcd	calcd	NOUN
eurjchem-1369	295	4	.	.	PUNCT
eurjchem-1369	296	1	for	for	ADP
eurjchem-1369	296	2	c12h15n7o5	c12h15n7o5	PROPN
eurjchem-1369	296	3	:	:	PUNCT
eurjchem-1369	296	4	c	c	X
eurjchem-1369	296	5	,	,	PUNCT
eurjchem-1369	296	6	42.73	42.73	NUM
eurjchem-1369	296	7	;	;	PUNCT
eurjchem-1369	296	8	h	h	NOUN
eurjchem-1369	296	9	,	,	PUNCT
eurjchem-1369	296	10	4.48	4.48	NUM
eurjchem-1369	296	11	;	;	PUNCT
eurjchem-1369	296	12	n	n	CCONJ
eurjchem-1369	296	13	,	,	PUNCT
eurjchem-1369	296	14	29.07	29.07	NUM
eurjchem-1369	296	15	.	.	PUNCT
eurjchem-1369	296	16	found	find	VERB
eurjchem-1369	296	17	:	:	PUNCT
eurjchem-1369	297	1	c	c	X
eurjchem-1369	297	2	,	,	PUNCT
eurjchem-1369	297	3	42.55	42.55	NUM
eurjchem-1369	297	4	;	;	PUNCT
eurjchem-1369	297	5	h	h	NOUN
eurjchem-1369	297	6	,	,	PUNCT
eurjchem-1369	297	7	4.65	4.65	NUM
eurjchem-1369	297	8	;	;	PUNCT
eurjchem-1369	297	9	n	n	CCONJ
eurjchem-1369	297	10	,	,	PUNCT
eurjchem-1369	297	11	29.25	29.25	NUM
eurjchem-1369	297	12	%	%	NOUN
eurjchem-1369	297	13	.	.	PUNCT
eurjchem-1369	298	1	4‐amino‐3‐cyano‐7‐ureido‐pyrazolo[5	4‐amino‐3‐cyano‐7‐ureido‐pyrazolo[5	NUM
eurjchem-1369	298	2	,	,	PUNCT
eurjchem-1369	298	3	1‐c][1,2,4]triazine‐8‐	1‐c][1,2,4]triazine‐8‐	PROPN
eurjchem-1369	298	4	carboxylic	carboxylic	ADJ
eurjchem-1369	298	5	acid	acid	NOUN
eurjchem-1369	298	6	ethyl	ethyl	PROPN
eurjchem-1369	298	7	ester	ester	NOUN
eurjchem-1369	298	8	(	(	PUNCT
eurjchem-1369	298	9	22b	22b	NUM
eurjchem-1369	298	10	):	):	PUNCT
eurjchem-1369	298	11	color	color	NOUN
eurjchem-1369	298	12	:	:	PUNCT
eurjchem-1369	298	13	yellow	yellow	ADJ
eurjchem-1369	298	14	crystals	crystal	NOUN
eurjchem-1369	298	15	.	.	PUNCT
eurjchem-1369	299	1	yield	yield	NOUN
eurjchem-1369	299	2	:	:	PUNCT
eurjchem-1369	299	3	72	72	NUM
eurjchem-1369	299	4	%	%	NOUN
eurjchem-1369	299	5	.	.	PUNCT
eurjchem-1369	300	1	m.p	m.p	PROPN
eurjchem-1369	300	2	.	.	PROPN
eurjchem-1369	300	3	:	:	PUNCT
eurjchem-1369	301	1	310‐312	310‐312	NUM
eurjchem-1369	301	2	°	°	NOUN
eurjchem-1369	301	3	c	c	X
eurjchem-1369	301	4	.	.	PUNCT
eurjchem-1369	301	5	ft‐ir	ft‐ir	NOUN
eurjchem-1369	301	6	(	(	PUNCT
eurjchem-1369	301	7	kbr	kbr	PROPN
eurjchem-1369	301	8	,	,	PUNCT
eurjchem-1369	301	9			PROPN
eurjchem-1369	301	10	,	,	PUNCT
eurjchem-1369	301	11	cm‐1	cm‐1	PROPN
eurjchem-1369	301	12	):	):	PUNCT
eurjchem-1369	301	13	3385‐3326	3385‐3326	NUM
eurjchem-1369	301	14	(	(	PUNCT
eurjchem-1369	301	15	nh2	nh2	PROPN
eurjchem-1369	301	16	)	)	PUNCT
eurjchem-1369	301	17	,	,	PUNCT
eurjchem-1369	301	18	3277	3277	NUM
eurjchem-1369	301	19	(	(	PUNCT
eurjchem-1369	301	20	nh	nh	NOUN
eurjchem-1369	301	21	)	)	PUNCT
eurjchem-1369	301	22	,	,	PUNCT
eurjchem-1369	301	23	2215	2215	NUM
eurjchem-1369	301	24	(	(	PUNCT
eurjchem-1369	301	25	cn	cn	PROPN
eurjchem-1369	301	26	)	)	PUNCT
eurjchem-1369	301	27	,	,	PUNCT
eurjchem-1369	301	28	1704	1704	NUM
eurjchem-1369	301	29	,	,	PUNCT
eurjchem-1369	301	30	1682	1682	NUM
eurjchem-1369	301	31	(	(	PUNCT
eurjchem-1369	301	32	c	c	X
eurjchem-1369	301	33	=	=	SYM
eurjchem-1369	301	34	o	o	NOUN
eurjchem-1369	301	35	's	's	PART
eurjchem-1369	301	36	)	)	PUNCT
eurjchem-1369	301	37	.	.	PUNCT
eurjchem-1369	302	1	1h	1h	NUM
eurjchem-1369	302	2	nmr	nmr	NOUN
eurjchem-1369	302	3	(	(	PUNCT
eurjchem-1369	302	4	250	250	NUM
eurjchem-1369	302	5	mhz	mhz	NOUN
eurjchem-1369	302	6	,	,	PUNCT
eurjchem-1369	302	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	302	8	,	,	PUNCT
eurjchem-1369	302	9	δ	δ	PROPN
eurjchem-1369	302	10	,	,	PUNCT
eurjchem-1369	302	11	ppm	ppm	NUM
eurjchem-1369	302	12	):	):	PUNCT
eurjchem-1369	302	13	1.15‐1.32	1.15‐1.32	NUM
eurjchem-1369	302	14	(	(	PUNCT
eurjchem-1369	302	15	t	t	PROPN
eurjchem-1369	302	16	,	,	PUNCT
eurjchem-1369	302	17	3h	3h	NUM
eurjchem-1369	302	18	,	,	PUNCT
eurjchem-1369	302	19	ch3	ch3	PROPN
eurjchem-1369	302	20	)	)	PUNCT
eurjchem-1369	302	21	,	,	PUNCT
eurjchem-1369	302	22	4.20‐4.35	4.20‐4.35	NUM
eurjchem-1369	302	23	(	(	PUNCT
eurjchem-1369	302	24	q	q	NOUN
eurjchem-1369	302	25	,	,	PUNCT
eurjchem-1369	302	26	2h	2h	NUM
eurjchem-1369	302	27	,	,	PUNCT
eurjchem-1369	302	28	‐ch2	‐ch2	NUM
eurjchem-1369	302	29	)	)	PUNCT
eurjchem-1369	302	30	,	,	PUNCT
eurjchem-1369	302	31	6.58	6.58	NUM
eurjchem-1369	302	32	(	(	PUNCT
eurjchem-1369	302	33	s	s	PROPN
eurjchem-1369	302	34	,	,	PUNCT
eurjchem-1369	302	35	2h	2h	NUM
eurjchem-1369	302	36	,	,	PUNCT
eurjchem-1369	302	37	nh2	nh2	PROPN
eurjchem-1369	302	38	)	)	PUNCT
eurjchem-1369	302	39	,	,	PUNCT
eurjchem-1369	302	40	7.37	7.37	NUM
eurjchem-1369	302	41	(	(	PUNCT
eurjchem-1369	302	42	s	s	PROPN
eurjchem-1369	302	43	,	,	PUNCT
eurjchem-1369	302	44	2h	2h	NUM
eurjchem-1369	302	45	,	,	PUNCT
eurjchem-1369	302	46	nh2	nh2	PROPN
eurjchem-1369	302	47	)	)	PUNCT
eurjchem-1369	302	48	,	,	PUNCT
eurjchem-1369	302	49	8.38	8.38	NUM
eurjchem-1369	302	50	(	(	PUNCT
eurjchem-1369	302	51	s	s	PROPN
eurjchem-1369	302	52	,	,	PUNCT
eurjchem-1369	302	53	1h	1h	NUM
eurjchem-1369	302	54	,	,	PUNCT
eurjchem-1369	302	55	nh	nh	PROPN
eurjchem-1369	302	56	)	)	PUNCT
eurjchem-1369	302	57	.	.	PUNCT
eurjchem-1369	303	1	ms	ms	NOUN
eurjchem-1369	303	2	(	(	PUNCT
eurjchem-1369	303	3	ei	ei	PROPN
eurjchem-1369	303	4	,	,	PUNCT
eurjchem-1369	303	5	m	m	PROPN
eurjchem-1369	303	6	/	/	SYM
eurjchem-1369	303	7	z	z	PROPN
eurjchem-1369	303	8	(	(	PUNCT
eurjchem-1369	303	9	%	%	NOUN
eurjchem-1369	303	10	)	)	PUNCT
eurjchem-1369	303	11	):	):	PUNCT
eurjchem-1369	303	12	290	290	NUM
eurjchem-1369	303	13	(	(	PUNCT
eurjchem-1369	303	14	m+	m+	NUM
eurjchem-1369	303	15	,	,	PUNCT
eurjchem-1369	303	16	8)	8)	NUM
eurjchem-1369	303	17	.	.	PUNCT
eurjchem-1369	303	18	anal	anal	PROPN
eurjchem-1369	303	19	.	.	PUNCT
eurjchem-1369	303	20	calcd	calcd	NOUN
eurjchem-1369	303	21	.	.	PUNCT
eurjchem-1369	304	1	for	for	ADP
eurjchem-1369	304	2	c10h10n8o3	c10h10n8o3	PROPN
eurjchem-1369	304	3	:	:	PUNCT
eurjchem-1369	304	4	c	c	X
eurjchem-1369	304	5	,	,	PUNCT
eurjchem-1369	304	6	41.38	41.38	NUM
eurjchem-1369	304	7	;	;	PUNCT
eurjchem-1369	304	8	h	h	NOUN
eurjchem-1369	304	9	,	,	PUNCT
eurjchem-1369	304	10	3.47	3.47	NUM
eurjchem-1369	304	11	;	;	PUNCT
eurjchem-1369	304	12	n	n	CCONJ
eurjchem-1369	304	13	,	,	PUNCT
eurjchem-1369	304	14	38.61	38.61	NUM
eurjchem-1369	304	15	.	.	PUNCT
eurjchem-1369	304	16	found	find	VERB
eurjchem-1369	304	17	:	:	PUNCT
eurjchem-1369	305	1	c	c	X
eurjchem-1369	305	2	,	,	PUNCT
eurjchem-1369	305	3	41.66	41.66	NUM
eurjchem-1369	305	4	;	;	PUNCT
eurjchem-1369	305	5	h	h	NOUN
eurjchem-1369	305	6	,	,	PUNCT
eurjchem-1369	305	7	3.54	3.54	NUM
eurjchem-1369	305	8	;	;	PUNCT
eurjchem-1369	305	9	n	n	CCONJ
eurjchem-1369	305	10	,	,	PUNCT
eurjchem-1369	305	11	38.72	38.72	NUM
eurjchem-1369	305	12	%	%	NOUN
eurjchem-1369	305	13	.	.	PUNCT
eurjchem-1369	306	1	2.2.12	2.2.12	NUM
eurjchem-1369	306	2	.	.	PUNCT
eurjchem-1369	306	3	16‐ureido‐11,12,14,15‐tetraaza‐cyclopenta[a	16‐ureido‐11,12,14,15‐tetraaza‐cyclopenta[a	X
eurjchem-1369	306	4	]	]	X
eurjchem-1369	306	5	phenanthrene‐17‐carboxylic	phenanthrene‐17‐carboxylic	ADJ
eurjchem-1369	306	6	acid	acid	PROPN
eurjchem-1369	306	7	ethyl	ethyl	PROPN
eurjchem-1369	306	8	ester	ester	NOUN
eurjchem-1369	306	9	(	(	PUNCT
eurjchem-1369	306	10	19	19	NUM
eurjchem-1369	306	11	)	)	PUNCT
eurjchem-1369	306	12	to	to	ADP
eurjchem-1369	306	13	a	a	DET
eurjchem-1369	306	14	solution	solution	NOUN
eurjchem-1369	306	15	of	of	ADP
eurjchem-1369	306	16	compound	compound	NOUN
eurjchem-1369	306	17	18	18	NUM
eurjchem-1369	306	18	(	(	PUNCT
eurjchem-1369	306	19	3.68	3.68	NUM
eurjchem-1369	306	20	g	g	NOUN
eurjchem-1369	306	21	,	,	PUNCT
eurjchem-1369	306	22	0.01	0.01	NUM
eurjchem-1369	306	23	mol	mol	NOUN
eurjchem-1369	306	24	)	)	PUNCT
eurjchem-1369	306	25	in	in	ADP
eurjchem-1369	306	26	acetic	acetic	ADJ
eurjchem-1369	306	27	acid	acid	NOUN
eurjchem-1369	306	28	(	(	PUNCT
eurjchem-1369	306	29	20	20	NUM
eurjchem-1369	306	30	ml	ml	NOUN
eurjchem-1369	306	31	)	)	PUNCT
eurjchem-1369	306	32	was	be	AUX
eurjchem-1369	306	33	heated	heat	VERB
eurjchem-1369	306	34	under	under	ADP
eurjchem-1369	306	35	reflux	reflux	NOUN
eurjchem-1369	306	36	for	for	ADP
eurjchem-1369	306	37	3	3	NUM
eurjchem-1369	306	38	h.	h.	NOUN
eurjchem-1369	306	39	the	the	DET
eurjchem-1369	306	40	solvent	solvent	NOUN
eurjchem-1369	306	41	was	be	AUX
eurjchem-1369	306	42	then	then	ADV
eurjchem-1369	306	43	evaporated	evaporate	VERB
eurjchem-1369	306	44	in	in	ADP
eurjchem-1369	306	45	vacuo	vacuo	NOUN
eurjchem-1369	306	46	,	,	PUNCT
eurjchem-1369	306	47	and	and	CCONJ
eurjchem-1369	306	48	the	the	DET
eurjchem-1369	306	49	remaining	remain	VERB
eurjchem-1369	306	50	solid	solid	ADJ
eurjchem-1369	306	51	product	product	NOUN
eurjchem-1369	306	52	was	be	AUX
eurjchem-1369	306	53	crystallized	crystallize	VERB
eurjchem-1369	306	54	from	from	ADP
eurjchem-1369	306	55	dimethylformamide	dimethylformamide	NOUN
eurjchem-1369	306	56	(	(	PUNCT
eurjchem-1369	306	57	scheme	scheme	NOUN
eurjchem-1369	306	58	5	5	NUM
eurjchem-1369	306	59	)	)	PUNCT
eurjchem-1369	306	60	.	.	PUNCT
eurjchem-1369	307	1	color	color	NOUN
eurjchem-1369	307	2	:	:	PUNCT
eurjchem-1369	307	3	red	red	ADJ
eurjchem-1369	307	4	crystals	crystal	NOUN
eurjchem-1369	307	5	.	.	PUNCT
eurjchem-1369	308	1	yield	yield	NOUN
eurjchem-1369	308	2	:	:	PUNCT
eurjchem-1369	308	3	77	77	NUM
eurjchem-1369	308	4	%	%	NOUN
eurjchem-1369	308	5	.	.	PUNCT
eurjchem-1369	309	1	m.p	m.p	PROPN
eurjchem-1369	309	2	.	.	PROPN
eurjchem-1369	309	3	:	:	PUNCT
eurjchem-1369	310	1	330‐332	330‐332	PROPN
eurjchem-1369	310	2	°	°	PROPN
eurjchem-1369	310	3	c	c	X
eurjchem-1369	310	4	.	.	PUNCT
eurjchem-1369	311	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	311	2	(	(	PUNCT
eurjchem-1369	311	3	kbr	kbr	PROPN
eurjchem-1369	311	4	,	,	PUNCT
eurjchem-1369	311	5			PROPN
eurjchem-1369	311	6	,	,	PUNCT
eurjchem-1369	311	7	cm‐1	cm‐1	PROPN
eurjchem-1369	311	8	):	):	PUNCT
eurjchem-1369	311	9	3445‐3326	3445‐3326	NUM
eurjchem-1369	311	10	(	(	PUNCT
eurjchem-1369	311	11	nh2	nh2	PROPN
eurjchem-1369	311	12	)	)	PUNCT
eurjchem-1369	311	13	,	,	PUNCT
eurjchem-1369	311	14	3165	3165	NUM
eurjchem-1369	311	15	(	(	PUNCT
eurjchem-1369	311	16	nh	nh	NOUN
eurjchem-1369	311	17	)	)	PUNCT
eurjchem-1369	311	18	,	,	PUNCT
eurjchem-1369	311	19	1715	1715	NUM
eurjchem-1369	311	20	,	,	PUNCT
eurjchem-1369	311	21	1695	1695	NUM
eurjchem-1369	311	22	(	(	PUNCT
eurjchem-1369	311	23	c	c	X
eurjchem-1369	311	24	=	=	SYM
eurjchem-1369	311	25	o	o	NOUN
eurjchem-1369	311	26	's	's	PART
eurjchem-1369	311	27	)	)	PUNCT
eurjchem-1369	311	28	.	.	PUNCT
eurjchem-1369	312	1	1h	1h	NUM
eurjchem-1369	312	2	nmr	nmr	NOUN
eurjchem-1369	312	3	(	(	PUNCT
eurjchem-1369	312	4	250	250	NUM
eurjchem-1369	312	5	mhz	mhz	NOUN
eurjchem-1369	312	6	,	,	PUNCT
eurjchem-1369	312	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	312	8	,	,	PUNCT
eurjchem-1369	312	9	δ	δ	PROPN
eurjchem-1369	312	10	,	,	PUNCT
eurjchem-1369	312	11	ppm	ppm	NOUN
eurjchem-1369	312	12	):	):	PUNCT
eurjchem-1369	312	13	1.24‐1.35	1.24‐1.35	NUM
eurjchem-1369	312	14	(	(	PUNCT
eurjchem-1369	312	15	t	t	PROPN
eurjchem-1369	312	16	,	,	PUNCT
eurjchem-1369	312	17	3h	3h	NUM
eurjchem-1369	312	18	,	,	PUNCT
eurjchem-1369	312	19	ch3	ch3	PROPN
eurjchem-1369	312	20	)	)	PUNCT
eurjchem-1369	312	21	,	,	PUNCT
eurjchem-1369	312	22	4.15‐4.37	4.15‐4.37	NUM
eurjchem-1369	312	23	(	(	PUNCT
eurjchem-1369	312	24	q	q	NOUN
eurjchem-1369	312	25	,	,	PUNCT
eurjchem-1369	312	26	2h	2h	NUM
eurjchem-1369	312	27	,	,	PUNCT
eurjchem-1369	312	28	ch2	ch2	PROPN
eurjchem-1369	312	29	)	)	PUNCT
eurjchem-1369	312	30	,	,	PUNCT
eurjchem-1369	312	31	6.95	6.95	NUM
eurjchem-1369	312	32	(	(	PUNCT
eurjchem-1369	312	33	s	s	NOUN
eurjchem-1369	312	34	,	,	PUNCT
eurjchem-1369	312	35	2h	2h	NUM
eurjchem-1369	312	36	,	,	PUNCT
eurjchem-1369	312	37	nh2	nh2	PROPN
eurjchem-1369	312	38	)	)	PUNCT
eurjchem-1369	312	39	,	,	PUNCT
eurjchem-1369	312	40	7.15‐8.25	7.15‐8.25	NUM
eurjchem-1369	312	41	(	(	PUNCT
eurjchem-1369	312	42	m	m	PROPN
eurjchem-1369	312	43	,	,	PUNCT
eurjchem-1369	312	44	6h	6h	NUM
eurjchem-1369	312	45	,	,	PUNCT
eurjchem-1369	312	46	ar‐h	ar‐h	PROPN
eurjchem-1369	312	47	)	)	PUNCT
eurjchem-1369	312	48	,	,	PUNCT
eurjchem-1369	312	49	8.87	8.87	NUM
eurjchem-1369	312	50	(	(	PUNCT
eurjchem-1369	312	51	s	s	PROPN
eurjchem-1369	312	52	,	,	PUNCT
eurjchem-1369	312	53	1h	1h	NUM
eurjchem-1369	312	54	,	,	PUNCT
eurjchem-1369	312	55	nh	nh	PROPN
eurjchem-1369	312	56	)	)	PUNCT
eurjchem-1369	312	57	.	.	PUNCT
eurjchem-1369	313	1	ms	ms	NOUN
eurjchem-1369	313	2	(	(	PUNCT
eurjchem-1369	313	3	ei	ei	PROPN
eurjchem-1369	313	4	,	,	PUNCT
eurjchem-1369	313	5	m	m	PROPN
eurjchem-1369	313	6	/	/	SYM
eurjchem-1369	313	7	z	z	PROPN
eurjchem-1369	313	8	(	(	PUNCT
eurjchem-1369	313	9	%	%	NOUN
eurjchem-1369	313	10	)	)	PUNCT
eurjchem-1369	313	11	):	):	PUNCT
eurjchem-1369	313	12	350	350	NUM
eurjchem-1369	313	13	(	(	PUNCT
eurjchem-1369	313	14	m+	m+	NUM
eurjchem-1369	313	15	,	,	PUNCT
eurjchem-1369	313	16	100	100	NUM
eurjchem-1369	313	17	)	)	PUNCT
eurjchem-1369	313	18	.	.	PUNCT
eurjchem-1369	314	1	anal	anal	PROPN
eurjchem-1369	314	2	.	.	PUNCT
eurjchem-1369	314	3	calcd	calcd	NOUN
eurjchem-1369	314	4	.	.	PUNCT
eurjchem-1369	315	1	for	for	SCONJ
eurjchem-1369	315	2	c17h14n6o3	c17h14n6o3	PROPN
eurjchem-1369	315	3	:	:	PUNCT
eurjchem-1369	315	4	c	c	X
eurjchem-1369	315	5	,	,	PUNCT
eurjchem-1369	315	6	58.28	58.28	NUM
eurjchem-1369	315	7	;	;	PUNCT
eurjchem-1369	315	8	h	h	NOUN
eurjchem-1369	315	9	,	,	PUNCT
eurjchem-1369	315	10	4.03	4.03	NUM
eurjchem-1369	315	11	;	;	PUNCT
eurjchem-1369	315	12	n	n	CCONJ
eurjchem-1369	315	13	,	,	PUNCT
eurjchem-1369	315	14	23.99	23.99	NUM
eurjchem-1369	315	15	.	.	PUNCT
eurjchem-1369	315	16	found	find	VERB
eurjchem-1369	315	17	:	:	PUNCT
eurjchem-1369	316	1	c	c	X
eurjchem-1369	316	2	,	,	PUNCT
eurjchem-1369	316	3	58.45	58.45	NUM
eurjchem-1369	316	4	;	;	PUNCT
eurjchem-1369	316	5	h	h	NOUN
eurjchem-1369	316	6	,	,	PUNCT
eurjchem-1369	316	7	4.24	4.24	NUM
eurjchem-1369	316	8	;	;	PUNCT
eurjchem-1369	316	9	n	n	CCONJ
eurjchem-1369	316	10	,	,	PUNCT
eurjchem-1369	316	11	23.72	23.72	NUM
eurjchem-1369	316	12	%	%	NOUN
eurjchem-1369	316	13	.	.	PUNCT
eurjchem-1369	317	1	112	112	NUM
eurjchem-1369	317	2	abbas‐temirek	abbas‐temirek	NOUN
eurjchem-1369	317	3	and	and	CCONJ
eurjchem-1369	317	4	abo‐bakr	abo‐bakr	ADJ
eurjchem-1369	317	5	/	/	SYM
eurjchem-1369	317	6	european	european	ADJ
eurjchem-1369	317	7	journal	journal	PROPN
eurjchem-1369	317	8	of	of	ADP
eurjchem-1369	317	9	chemistry	chemistry	NOUN
eurjchem-1369	317	10	7	7	NUM
eurjchem-1369	317	11	(	(	PUNCT
eurjchem-1369	317	12	1	1	NUM
eurjchem-1369	317	13	)	)	PUNCT
eurjchem-1369	317	14	(	(	PUNCT
eurjchem-1369	317	15	2016	2016	NUM
eurjchem-1369	317	16	)	)	PUNCT
eurjchem-1369	318	1	107‐114	107‐114	NUM
eurjchem-1369	318	2	scheme	scheme	NOUN
eurjchem-1369	318	3	5	5	NUM
eurjchem-1369	318	4	2.2.13	2.2.13	NUM
eurjchem-1369	318	5	.	.	PUNCT
eurjchem-1369	319	1	8‐hydroxy‐2‐ureido‐benzo[e]pyrazolo[5,1‐c][1,2,4	8‐hydroxy‐2‐ureido‐benzo[e]pyrazolo[5,1‐c][1,2,4	NUM
eurjchem-1369	319	2	]	]	X
eurjchem-1369	319	3	triazine‐3‐carboxylic	triazine‐3‐carboxylic	NUM
eurjchem-1369	319	4	acid	acid	PROPN
eurjchem-1369	319	5	ethyl	ethyl	PROPN
eurjchem-1369	319	6	ester	ester	NOUN
eurjchem-1369	319	7	(	(	PUNCT
eurjchem-1369	319	8	21	21	NUM
eurjchem-1369	319	9	)	)	PUNCT
eurjchem-1369	319	10	to	to	ADP
eurjchem-1369	319	11	a	a	DET
eurjchem-1369	319	12	solution	solution	NOUN
eurjchem-1369	319	13	of	of	ADP
eurjchem-1369	319	14	compound	compound	NOUN
eurjchem-1369	319	15	20	20	NUM
eurjchem-1369	319	16	(	(	PUNCT
eurjchem-1369	319	17	3.34	3.34	NUM
eurjchem-1369	319	18	g	g	NOUN
eurjchem-1369	319	19	,	,	PUNCT
eurjchem-1369	319	20	0.01	0.01	NUM
eurjchem-1369	319	21	mol	mol	NOUN
eurjchem-1369	319	22	)	)	PUNCT
eurjchem-1369	319	23	in	in	ADP
eurjchem-1369	319	24	acetic	acetic	ADJ
eurjchem-1369	319	25	acid	acid	NOUN
eurjchem-1369	319	26	(	(	PUNCT
eurjchem-1369	319	27	20	20	NUM
eurjchem-1369	319	28	ml	ml	NOUN
eurjchem-1369	319	29	)	)	PUNCT
eurjchem-1369	319	30	was	be	AUX
eurjchem-1369	319	31	heated	heat	VERB
eurjchem-1369	319	32	under	under	ADP
eurjchem-1369	319	33	reflux	reflux	NOUN
eurjchem-1369	319	34	for	for	ADP
eurjchem-1369	319	35	4	4	NUM
eurjchem-1369	319	36	hrs	hrs	NOUN
eurjchem-1369	319	37	.	.	PUNCT
eurjchem-1369	320	1	the	the	DET
eurjchem-1369	320	2	solvent	solvent	NOUN
eurjchem-1369	320	3	was	be	AUX
eurjchem-1369	320	4	then	then	ADV
eurjchem-1369	320	5	evaporated	evaporate	VERB
eurjchem-1369	320	6	in	in	ADP
eurjchem-1369	320	7	vacuo	vacuo	NOUN
eurjchem-1369	320	8	,	,	PUNCT
eurjchem-1369	320	9	and	and	CCONJ
eurjchem-1369	320	10	the	the	DET
eurjchem-1369	320	11	remaining	remain	VERB
eurjchem-1369	320	12	solid	solid	ADJ
eurjchem-1369	320	13	product	product	NOUN
eurjchem-1369	320	14	was	be	AUX
eurjchem-1369	320	15	crystallized	crystallize	VERB
eurjchem-1369	320	16	from	from	ADP
eurjchem-1369	320	17	dimethylformamide	dimethylformamide	NOUN
eurjchem-1369	320	18	(	(	PUNCT
eurjchem-1369	320	19	scheme	scheme	NOUN
eurjchem-1369	320	20	5	5	NUM
eurjchem-1369	320	21	)	)	PUNCT
eurjchem-1369	320	22	.	.	PUNCT
eurjchem-1369	321	1	color	color	NOUN
eurjchem-1369	321	2	:	:	PUNCT
eurjchem-1369	321	3	yellow	yellow	ADJ
eurjchem-1369	321	4	crystals	crystal	NOUN
eurjchem-1369	321	5	.	.	PUNCT
eurjchem-1369	322	1	yield	yield	NOUN
eurjchem-1369	322	2	:	:	PUNCT
eurjchem-1369	322	3	85	85	NUM
eurjchem-1369	322	4	%	%	NOUN
eurjchem-1369	322	5	.	.	PUNCT
eurjchem-1369	323	1	m.p	m.p	PROPN
eurjchem-1369	323	2	.	.	PROPN
eurjchem-1369	323	3	:	:	PUNCT
eurjchem-1369	324	1	368‐370	368‐370	NUM
eurjchem-1369	324	2	°	°	PROPN
eurjchem-1369	324	3	c	c	X
eurjchem-1369	324	4	.	.	PUNCT
eurjchem-1369	325	1	ft‐ir	ft‐ir	NOUN
eurjchem-1369	325	2	(	(	PUNCT
eurjchem-1369	325	3	kbr	kbr	PROPN
eurjchem-1369	325	4	,	,	PUNCT
eurjchem-1369	325	5			PROPN
eurjchem-1369	325	6	,	,	PUNCT
eurjchem-1369	325	7	cm‐1	cm‐1	PROPN
eurjchem-1369	325	8	):	):	PUNCT
eurjchem-1369	325	9	3445‐3326	3445‐3326	NUM
eurjchem-1369	325	10	(	(	PUNCT
eurjchem-1369	325	11	nh2	nh2	NOUN
eurjchem-1369	325	12	and	and	CCONJ
eurjchem-1369	325	13	oh	oh	INTJ
eurjchem-1369	325	14	)	)	PUNCT
eurjchem-1369	325	15	,	,	PUNCT
eurjchem-1369	325	16	3165	3165	NUM
eurjchem-1369	325	17	(	(	PUNCT
eurjchem-1369	325	18	nh	nh	NOUN
eurjchem-1369	325	19	)	)	PUNCT
eurjchem-1369	325	20	,	,	PUNCT
eurjchem-1369	325	21	1715	1715	NUM
eurjchem-1369	325	22	,	,	PUNCT
eurjchem-1369	325	23	1695	1695	NUM
eurjchem-1369	325	24	(	(	PUNCT
eurjchem-1369	325	25	c	c	X
eurjchem-1369	325	26	=	=	SYM
eurjchem-1369	325	27	o	o	NOUN
eurjchem-1369	325	28	's	's	PART
eurjchem-1369	325	29	)	)	PUNCT
eurjchem-1369	325	30	.	.	PUNCT
eurjchem-1369	326	1	1h	1h	NUM
eurjchem-1369	326	2	nmr	nmr	NOUN
eurjchem-1369	326	3	(	(	PUNCT
eurjchem-1369	326	4	250	250	NUM
eurjchem-1369	326	5	mhz	mhz	NOUN
eurjchem-1369	326	6	,	,	PUNCT
eurjchem-1369	326	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1369	326	8	,	,	PUNCT
eurjchem-1369	326	9	δ	δ	PROPN
eurjchem-1369	326	10	,	,	PUNCT
eurjchem-1369	326	11	ppm	ppm	NUM
eurjchem-1369	326	12	):	):	PUNCT
eurjchem-1369	326	13	1.17‐1.31	1.17‐1.31	PROPN
eurjchem-1369	326	14	(	(	PUNCT
eurjchem-1369	326	15	t	t	PROPN
eurjchem-1369	326	16	,	,	PUNCT
eurjchem-1369	326	17	3h	3h	NUM
eurjchem-1369	326	18	,	,	PUNCT
eurjchem-1369	326	19	ch3	ch3	PROPN
eurjchem-1369	326	20	)	)	PUNCT
eurjchem-1369	326	21	,	,	PUNCT
eurjchem-1369	326	22	4.14‐4.36	4.14‐4.36	NUM
eurjchem-1369	326	23	(	(	PUNCT
eurjchem-1369	326	24	q	q	NOUN
eurjchem-1369	326	25	,	,	PUNCT
eurjchem-1369	326	26	2h	2h	NUM
eurjchem-1369	326	27	,	,	PUNCT
eurjchem-1369	326	28	ch2	ch2	PROPN
eurjchem-1369	326	29	)	)	PUNCT
eurjchem-1369	326	30	,	,	PUNCT
eurjchem-1369	326	31	6.65	6.65	NUM
eurjchem-1369	326	32	(	(	PUNCT
eurjchem-1369	326	33	s	s	NOUN
eurjchem-1369	326	34	,	,	PUNCT
eurjchem-1369	326	35	2h	2h	NUM
eurjchem-1369	326	36	,	,	PUNCT
eurjchem-1369	326	37	nh2	nh2	PROPN
eurjchem-1369	326	38	)	)	PUNCT
eurjchem-1369	326	39	,	,	PUNCT
eurjchem-1369	326	40	7.14‐7.88	7.14‐7.88	NUM
eurjchem-1369	326	41	(	(	PUNCT
eurjchem-1369	326	42	m	m	PROPN
eurjchem-1369	326	43	,	,	PUNCT
eurjchem-1369	326	44	3h	3h	NUM
eurjchem-1369	326	45	,	,	PUNCT
eurjchem-1369	326	46	ar‐h	ar‐h	NOUN
eurjchem-1369	326	47	)	)	PUNCT
eurjchem-1369	326	48	,	,	PUNCT
eurjchem-1369	326	49	9.10	9.10	NUM
eurjchem-1369	326	50	(	(	PUNCT
eurjchem-1369	326	51	s	s	PROPN
eurjchem-1369	326	52	,	,	PUNCT
eurjchem-1369	326	53	1h	1h	NUM
eurjchem-1369	326	54	,	,	PUNCT
eurjchem-1369	326	55	nh	nh	PROPN
eurjchem-1369	326	56	)	)	PUNCT
eurjchem-1369	326	57	,	,	PUNCT
eurjchem-1369	326	58	11.45	11.45	NUM
eurjchem-1369	326	59	(	(	PUNCT
eurjchem-1369	326	60	br.s	br.s	PROPN
eurjchem-1369	326	61	,	,	PUNCT
eurjchem-1369	326	62	1h	1h	NUM
eurjchem-1369	326	63	,	,	PUNCT
eurjchem-1369	326	64	oh	oh	INTJ
eurjchem-1369	326	65	)	)	PUNCT
eurjchem-1369	326	66	.	.	PUNCT
eurjchem-1369	327	1	ms	ms	NOUN
eurjchem-1369	327	2	(	(	PUNCT
eurjchem-1369	327	3	ei	ei	PROPN
eurjchem-1369	327	4	,	,	PUNCT
eurjchem-1369	327	5	m	m	PROPN
eurjchem-1369	327	6	/	/	SYM
eurjchem-1369	327	7	z	z	PROPN
eurjchem-1369	327	8	(	(	PUNCT
eurjchem-1369	327	9	%	%	NOUN
eurjchem-1369	327	10	)	)	PUNCT
eurjchem-1369	327	11	):	):	PUNCT
eurjchem-1369	327	12	316	316	NUM
eurjchem-1369	327	13	(	(	PUNCT
eurjchem-1369	327	14	m+	m+	NUM
eurjchem-1369	327	15	,	,	PUNCT
eurjchem-1369	327	16	19	19	NUM
eurjchem-1369	327	17	)	)	PUNCT
eurjchem-1369	327	18	.	.	PUNCT
eurjchem-1369	328	1	anal	anal	PROPN
eurjchem-1369	328	2	.	.	PUNCT
eurjchem-1369	328	3	calcd	calcd	NOUN
eurjchem-1369	328	4	.	.	PUNCT
eurjchem-1369	329	1	for	for	ADP
eurjchem-1369	329	2	c13h12n6o4	c13h12n6o4	PROPN
eurjchem-1369	329	3	:	:	PUNCT
eurjchem-1369	329	4	c	c	X
eurjchem-1369	329	5	,	,	PUNCT
eurjchem-1369	329	6	49.37	49.37	NUM
eurjchem-1369	329	7	;	;	PUNCT
eurjchem-1369	329	8	h	h	NOUN
eurjchem-1369	329	9	,	,	PUNCT
eurjchem-1369	329	10	3.82	3.82	NUM
eurjchem-1369	329	11	;	;	PUNCT
eurjchem-1369	329	12	n	n	CCONJ
eurjchem-1369	329	13	,	,	PUNCT
eurjchem-1369	329	14	26.57	26.57	NUM
eurjchem-1369	329	15	.	.	PUNCT
eurjchem-1369	329	16	found	find	VERB
eurjchem-1369	329	17	:	:	PUNCT
eurjchem-1369	330	1	c	c	X
eurjchem-1369	330	2	,	,	PUNCT
eurjchem-1369	330	3	49.45	49.45	NUM
eurjchem-1369	330	4	;	;	PUNCT
eurjchem-1369	330	5	h	h	X
eurjchem-1369	330	6	,	,	PUNCT
eurjchem-1369	330	7	3.64	3.64	NUM
eurjchem-1369	330	8	;	;	PUNCT
eurjchem-1369	330	9	n	n	CCONJ
eurjchem-1369	330	10	,	,	PUNCT
eurjchem-1369	330	11	26.75	26.75	NUM
eurjchem-1369	330	12	%	%	NOUN
eurjchem-1369	330	13	.	.	PUNCT
eurjchem-1369	331	1	3	3	X
eurjchem-1369	331	2	.	.	NOUN
eurjchem-1369	331	3	results	result	NOUN
eurjchem-1369	331	4	and	and	CCONJ
eurjchem-1369	331	5	discussion	discussion	NOUN
eurjchem-1369	331	6	3.1	3.1	NUM
eurjchem-1369	331	7	.	.	PUNCT
eurjchem-1369	332	1	chemistry	chemistry	NOUN
eurjchem-1369	332	2	the	the	DET
eurjchem-1369	332	3	reaction	reaction	NOUN
eurjchem-1369	332	4	of	of	ADP
eurjchem-1369	332	5	n‐bis(methylthio)methylenecyanamide	n‐bis(methylthio)methylenecyanamide	ADV
eurjchem-1369	332	6	(	(	PUNCT
eurjchem-1369	332	7	1	1	NUM
eurjchem-1369	332	8	)	)	PUNCT
eurjchem-1369	332	9	with	with	ADP
eurjchem-1369	332	10	ethylcyanoacetate	ethylcyanoacetate	NOUN
eurjchem-1369	332	11	or	or	CCONJ
eurjchem-1369	332	12	malononitrile	malononitrile	NOUN
eurjchem-1369	332	13	was	be	AUX
eurjchem-1369	332	14	conducted	conduct	VERB
eurjchem-1369	332	15	at	at	ADP
eurjchem-1369	332	16	room	room	NOUN
eurjchem-1369	332	17	temperature	temperature	NOUN
eurjchem-1369	332	18	in	in	ADP
eurjchem-1369	332	19	the	the	DET
eurjchem-1369	332	20	presence	presence	NOUN
eurjchem-1369	332	21	of	of	ADP
eurjchem-1369	332	22	potassium	potassium	NOUN
eurjchem-1369	332	23	carbonate	carbonate	NOUN
eurjchem-1369	332	24	in	in	ADP
eurjchem-1369	332	25	dimethysulfoxide	dimethysulfoxide	NOUN
eurjchem-1369	332	26	followed	follow	VERB
eurjchem-1369	332	27	by	by	ADP
eurjchem-1369	332	28	treatment	treatment	NOUN
eurjchem-1369	332	29	with	with	ADP
eurjchem-1369	332	30	10	10	NUM
eurjchem-1369	332	31	%	%	NOUN
eurjchem-1369	332	32	hydro‐	hydro‐	X
eurjchem-1369	332	33	chloric	chloric	NOUN
eurjchem-1369	332	34	acid	acid	PROPN
eurjchem-1369	332	35	,	,	PUNCT
eurjchem-1369	332	36	afforded	afford	VERB
eurjchem-1369	332	37	the	the	DET
eurjchem-1369	332	38	urea	urea	NOUN
eurjchem-1369	332	39	derivatives	derivative	NOUN
eurjchem-1369	332	40	3a	3a	NUM
eurjchem-1369	332	41	,	,	PUNCT
eurjchem-1369	332	42	b.	b.	PROPN
eurjchem-1369	333	1	this	this	PRON
eurjchem-1369	333	2	suggests	suggest	VERB
eurjchem-1369	333	3	that	that	SCONJ
eurjchem-1369	333	4	the	the	DET
eurjchem-1369	333	5	isolated	isolated	ADJ
eurjchem-1369	333	6	derivatives	derivative	NOUN
eurjchem-1369	333	7	3a	3a	NUM
eurjchem-1369	333	8	,	,	PUNCT
eurjchem-1369	333	9	b	b	PROPN
eurjchem-1369	333	10	were	be	AUX
eurjchem-1369	333	11	formed	form	VERB
eurjchem-1369	333	12	through	through	ADP
eurjchem-1369	333	13	the	the	DET
eurjchem-1369	333	14	intermediates	intermediate	NOUN
eurjchem-1369	333	15	2a	2a	NUM
eurjchem-1369	333	16	,	,	PUNCT
eurjchem-1369	333	17	b.	b.	PROPN
eurjchem-1369	333	18	the	the	DET
eurjchem-1369	333	19	ft‐ir	ft‐ir	NOUN
eurjchem-1369	333	20	spectrum	spectrum	NOUN
eurjchem-1369	333	21	showed	show	VERB
eurjchem-1369	333	22	the	the	DET
eurjchem-1369	333	23	presence	presence	NOUN
eurjchem-1369	333	24	of	of	ADP
eurjchem-1369	333	25	absorption	absorption	NOUN
eurjchem-1369	333	26	bands	band	NOUN
eurjchem-1369	333	27	of	of	ADP
eurjchem-1369	333	28	nh2	nh2	PROPN
eurjchem-1369	333	29	and	and	CCONJ
eurjchem-1369	333	30	nh	nh	NOUN
eurjchem-1369	333	31	groups	group	NOUN
eurjchem-1369	333	32	at	at	ADP
eurjchem-1369	333	33	3414	3414	NUM
eurjchem-1369	333	34	and	and	CCONJ
eurjchem-1369	333	35	3283	3283	NUM
eurjchem-1369	333	36	cm‐1	cm‐1	NOUN
eurjchem-1369	333	37	for	for	ADP
eurjchem-1369	333	38	compound	compound	NOUN
eurjchem-1369	333	39	3a	3a	NUM
eurjchem-1369	333	40	,	,	PUNCT
eurjchem-1369	333	41	and	and	CCONJ
eurjchem-1369	333	42	at	at	ADP
eurjchem-1369	333	43	3446	3446	NUM
eurjchem-1369	333	44	and	and	CCONJ
eurjchem-1369	333	45	3223	3223	NUM
eurjchem-1369	333	46	cm‐1	cm‐1	NOUN
eurjchem-1369	333	47	for	for	ADP
eurjchem-1369	333	48	compounds	compound	NOUN
eurjchem-1369	333	49	3b	3b	NUM
eurjchem-1369	333	50	,	,	PUNCT
eurjchem-1369	333	51	respectively	respectively	ADV
eurjchem-1369	333	52	.	.	PUNCT
eurjchem-1369	334	1	also	also	ADV
eurjchem-1369	334	2	,	,	PUNCT
eurjchem-1369	334	3	the	the	DET
eurjchem-1369	334	4	1h	1h	NUM
eurjchem-1369	334	5	nmr	nmr	NOUN
eurjchem-1369	334	6	spectrum	spectrum	NOUN
eurjchem-1369	334	7	showed	show	VERB
eurjchem-1369	334	8	the	the	DET
eurjchem-1369	334	9	presence	presence	NOUN
eurjchem-1369	334	10	of	of	ADP
eurjchem-1369	334	11	nh2	nh2	PROPN
eurjchem-1369	334	12	and	and	CCONJ
eurjchem-1369	334	13	nh	nh	NOUN
eurjchem-1369	334	14	groups	group	NOUN
eurjchem-1369	334	15	at	at	ADP
eurjchem-1369	334	16	δ	δ	PROPN
eurjchem-1369	334	17	7.07	7.07	NUM
eurjchem-1369	334	18	and	and	CCONJ
eurjchem-1369	334	19	10.21	10.21	NUM
eurjchem-1369	334	20	ppm	ppm	NOUN
eurjchem-1369	334	21	for	for	ADP
eurjchem-1369	334	22	compound	compound	NOUN
eurjchem-1369	334	23	3a	3a	PROPN
eurjchem-1369	334	24	and	and	CCONJ
eurjchem-1369	334	25	at	at	ADP
eurjchem-1369	334	26	δ	δ	PROPN
eurjchem-1369	334	27	7.60	7.60	NUM
eurjchem-1369	334	28	and	and	CCONJ
eurjchem-1369	334	29	10.95	10.95	NUM
eurjchem-1369	334	30	ppm	ppm	NOUN
eurjchem-1369	334	31	for	for	ADP
eurjchem-1369	334	32	compound	compound	NOUN
eurjchem-1369	334	33	3b	3b	NOUN
eurjchem-1369	334	34	,	,	PUNCT
eurjchem-1369	334	35	respectively	respectively	ADV
eurjchem-1369	334	36	.	.	PUNCT
eurjchem-1369	335	1	the	the	DET
eurjchem-1369	335	2	13c	13c	NUM
eurjchem-1369	335	3	nmr	nmr	NOUN
eurjchem-1369	335	4	of	of	ADP
eurjchem-1369	335	5	compounds	compound	NOUN
eurjchem-1369	335	6	3a	3a	NUM
eurjchem-1369	335	7	and	and	CCONJ
eurjchem-1369	335	8	3b	3b	NOUN
eurjchem-1369	335	9	showed	show	VERB
eurjchem-1369	335	10	eight	eight	NUM
eurjchem-1369	335	11	and	and	CCONJ
eurjchem-1369	335	12	six	six	NUM
eurjchem-1369	335	13	different	different	ADJ
eurjchem-1369	335	14	signals	signal	NOUN
eurjchem-1369	335	15	for	for	ADP
eurjchem-1369	335	16	eight	eight	NUM
eurjchem-1369	335	17	and	and	CCONJ
eurjchem-1369	335	18	six	six	NUM
eurjchem-1369	335	19	different	different	ADJ
eurjchem-1369	335	20	carbons	carbon	NOUN
eurjchem-1369	335	21	,	,	PUNCT
eurjchem-1369	335	22	respectively	respectively	ADV
eurjchem-1369	335	23	(	(	PUNCT
eurjchem-1369	335	24	scheme	scheme	NOUN
eurjchem-1369	335	25	1	1	NUM
eurjchem-1369	335	26	)	)	PUNCT
eurjchem-1369	335	27	.	.	PUNCT
eurjchem-1369	336	1	the	the	DET
eurjchem-1369	336	2	treatment	treatment	NOUN
eurjchem-1369	336	3	of	of	ADP
eurjchem-1369	336	4	compound	compound	NOUN
eurjchem-1369	336	5	3a	3a	NUM
eurjchem-1369	336	6	,	,	PUNCT
eurjchem-1369	336	7	b	b	NOUN
eurjchem-1369	336	8	with	with	ADP
eurjchem-1369	336	9	hydrazine	hydrazine	NOUN
eurjchem-1369	336	10	hydrate	hydrate	NOUN
eurjchem-1369	336	11	in	in	ADP
eurjchem-1369	336	12	ethanol	ethanol	NOUN
eurjchem-1369	336	13	afforded	afford	VERB
eurjchem-1369	336	14	the	the	DET
eurjchem-1369	336	15	corresponding	corresponding	ADJ
eurjchem-1369	336	16	aminopyrazole	aminopyrazole	NOUN
eurjchem-1369	336	17	derivatives	derivative	NOUN
eurjchem-1369	336	18	4a	4a	NOUN
eurjchem-1369	336	19	,	,	PUNCT
eurjchem-1369	336	20	b	b	X
eurjchem-1369	337	1	[	[	X
eurjchem-1369	337	2	20	20	NUM
eurjchem-1369	337	3	]	]	PUNCT
eurjchem-1369	337	4	(	(	PUNCT
eurjchem-1369	337	5	scheme	scheme	NOUN
eurjchem-1369	337	6	1	1	NUM
eurjchem-1369	337	7	)	)	PUNCT
eurjchem-1369	337	8	.	.	PUNCT
eurjchem-1369	338	1	the	the	DET
eurjchem-1369	338	2	chemical	chemical	NOUN
eurjchem-1369	338	3	structures	structure	NOUN
eurjchem-1369	338	4	of	of	ADP
eurjchem-1369	338	5	compounds	compound	NOUN
eurjchem-1369	338	6	4a	4a	NOUN
eurjchem-1369	338	7	and	and	CCONJ
eurjchem-1369	338	8	4b	4b	PROPN
eurjchem-1369	338	9	were	be	AUX
eurjchem-1369	338	10	in	in	ADP
eurjchem-1369	338	11	agreement	agreement	NOUN
eurjchem-1369	338	12	with	with	ADP
eurjchem-1369	338	13	their	their	PRON
eurjchem-1369	338	14	spectral	spectral	ADJ
eurjchem-1369	338	15	data	datum	NOUN
eurjchem-1369	338	16	and	and	CCONJ
eurjchem-1369	338	17	elemental	elemental	ADJ
eurjchem-1369	338	18	analyses	analysis	NOUN
eurjchem-1369	338	19	(	(	PUNCT
eurjchem-1369	338	20	experimental	experimental	ADJ
eurjchem-1369	338	21	part	part	NOUN
eurjchem-1369	338	22	)	)	PUNCT
eurjchem-1369	338	23	.	.	PUNCT
eurjchem-1369	339	1	the	the	DET
eurjchem-1369	339	2	13c	13c	NUM
eurjchem-1369	339	3	nmr	nmr	NOUN
eurjchem-1369	339	4	spectrum	spectrum	NOUN
eurjchem-1369	339	5	of	of	ADP
eurjchem-1369	339	6	compound	compound	NOUN
eurjchem-1369	339	7	4a	4a	NOUN
eurjchem-1369	339	8	showed	show	VERB
eurjchem-1369	339	9	the	the	DET
eurjchem-1369	339	10	presence	presence	NOUN
eurjchem-1369	339	11	of	of	ADP
eurjchem-1369	339	12	seven	seven	NUM
eurjchem-1369	339	13	different	different	ADJ
eurjchem-1369	339	14	signals	signal	NOUN
eurjchem-1369	339	15	corresponding	correspond	VERB
eurjchem-1369	339	16	to	to	ADP
eurjchem-1369	339	17	seven	seven	NUM
eurjchem-1369	339	18	different	different	ADJ
eurjchem-1369	339	19	carbons	carbon	NOUN
eurjchem-1369	339	20	at	at	ADP
eurjchem-1369	339	21	δ	δ	PROPN
eurjchem-1369	339	22	14.29	14.29	NUM
eurjchem-1369	339	23	(	(	PUNCT
eurjchem-1369	339	24	1c	1c	NOUN
eurjchem-1369	339	25	,	,	PUNCT
eurjchem-1369	339	26	ch3	ch3	PROPN
eurjchem-1369	339	27	)	)	PUNCT
eurjchem-1369	339	28	,	,	PUNCT
eurjchem-1369	339	29	14.60	14.60	NUM
eurjchem-1369	339	30	(=	(=	X
eurjchem-1369	339	31	c‐nh2	c‐nh2	PROPN
eurjchem-1369	339	32	)	)	PUNCT
eurjchem-1369	339	33	,	,	PUNCT
eurjchem-1369	339	34	38.69	38.69	NUM
eurjchem-1369	339	35	(	(	PUNCT
eurjchem-1369	339	36	n	n	CCONJ
eurjchem-1369	339	37	=	=	NOUN
eurjchem-1369	339	38	c‐nh	c‐nh	NOUN
eurjchem-1369	339	39	)	)	PUNCT
eurjchem-1369	339	40	,	,	PUNCT
eurjchem-1369	339	41	59.25	59.25	NUM
eurjchem-1369	339	42	(	(	PUNCT
eurjchem-1369	339	43	ch2	ch2	PROPN
eurjchem-1369	339	44	)	)	PUNCT
eurjchem-1369	339	45	,	,	PUNCT
eurjchem-1369	339	46	60.95	60.95	NUM
eurjchem-1369	339	47	(=	(=	NOUN
eurjchem-1369	339	48	c‐cooet	c‐cooet	VERB
eurjchem-1369	339	49	,	,	PUNCT
eurjchem-1369	339	50	154.59	154.59	NUM
eurjchem-1369	339	51	(	(	PUNCT
eurjchem-1369	339	52	conh2	conh2	PROPN
eurjchem-1369	339	53	)	)	PUNCT
eurjchem-1369	339	54	and	and	CCONJ
eurjchem-1369	339	55	at	at	ADP
eurjchem-1369	339	56	δ	δ	PROPN
eurjchem-1369	339	57	163.98	163.98	NUM
eurjchem-1369	339	58	ppm	ppm	NOUN
eurjchem-1369	339	59	(	(	PUNCT
eurjchem-1369	339	60	cooet	cooet	NOUN
eurjchem-1369	339	61	)	)	PUNCT
eurjchem-1369	339	62	,	,	PUNCT
eurjchem-1369	339	63	which	which	PRON
eurjchem-1369	339	64	proved	prove	VERB
eurjchem-1369	339	65	its	its	PRON
eurjchem-1369	339	66	structure	structure	NOUN
eurjchem-1369	339	67	.	.	PUNCT
eurjchem-1369	340	1	condensation	condensation	NOUN
eurjchem-1369	340	2	of	of	ADP
eurjchem-1369	340	3	compound	compound	NOUN
eurjchem-1369	340	4	4a	4a	NOUN
eurjchem-1369	340	5	with	with	ADP
eurjchem-1369	340	6	acetylacetone	acetylacetone	NOUN
eurjchem-1369	340	7	in	in	ADP
eurjchem-1369	340	8	acetic	acetic	ADJ
eurjchem-1369	340	9	acid	acid	NOUN
eurjchem-1369	340	10	yielded	yield	VERB
eurjchem-1369	340	11	5,7‐dimethyl‐2‐ureido‐pyrazolo[1,5‐a]pyrimidi‐	5,7‐dimethyl‐2‐ureido‐pyrazolo[1,5‐a]pyrimidi‐	NUM
eurjchem-1369	340	12	ne‐3‐carboxylic	ne‐3‐carboxylic	PROPN
eurjchem-1369	340	13	acid	acid	PROPN
eurjchem-1369	340	14	ethyl	ethyl	PROPN
eurjchem-1369	340	15	ester	ester	NOUN
eurjchem-1369	340	16	(	(	PUNCT
eurjchem-1369	340	17	5	5	NUM
eurjchem-1369	340	18	)	)	PUNCT
eurjchem-1369	340	19	.	.	PUNCT
eurjchem-1369	341	1	while	while	SCONJ
eurjchem-1369	341	2	the	the	DET
eurjchem-1369	341	3	reaction	reaction	NOUN
eurjchem-1369	341	4	of	of	ADP
eurjchem-1369	341	5	compound	compound	NOUN
eurjchem-1369	341	6	4a	4a	NOUN
eurjchem-1369	341	7	with	with	ADP
eurjchem-1369	341	8	ethyl	ethyl	PROPN
eurjchem-1369	341	9	acetoacetate	acetoacetate	NOUN
eurjchem-1369	341	10	or	or	CCONJ
eurjchem-1369	341	11	diethyl‐3‐oxoglutu‐	diethyl‐3‐oxoglutu‐	NOUN
eurjchem-1369	341	12	rate	rate	NOUN
eurjchem-1369	341	13	produced	produce	VERB
eurjchem-1369	341	14	the	the	DET
eurjchem-1369	341	15	corresponding	corresponding	PROPN
eurjchem-1369	341	16	pyrazolopyrimidine	pyrazolopyrimidine	PROPN
eurjchem-1369	341	17	derivati‐	derivati‐	X
eurjchem-1369	341	18	ves	ves	NUM
eurjchem-1369	341	19	6a	6a	NOUN
eurjchem-1369	341	20	,	,	PUNCT
eurjchem-1369	341	21	b	b	NOUN
eurjchem-1369	341	22	,	,	PUNCT
eurjchem-1369	341	23	respectively	respectively	ADV
eurjchem-1369	341	24	[	[	X
eurjchem-1369	341	25	21	21	NUM
eurjchem-1369	341	26	]	]	X
eurjchem-1369	341	27	(	(	PUNCT
eurjchem-1369	341	28	scheme	scheme	NOUN
eurjchem-1369	341	29	2	2	NUM
eurjchem-1369	341	30	)	)	PUNCT
eurjchem-1369	341	31	.	.	PUNCT
eurjchem-1369	342	1	the	the	DET
eurjchem-1369	342	2	elemental	elemental	ADJ
eurjchem-1369	342	3	analyses	analysis	NOUN
eurjchem-1369	342	4	and	and	CCONJ
eurjchem-1369	342	5	spectroscopic	spectroscopic	ADJ
eurjchem-1369	342	6	data	datum	NOUN
eurjchem-1369	342	7	are	be	AUX
eurjchem-1369	342	8	in	in	ADP
eurjchem-1369	342	9	consistent	consistent	ADJ
eurjchem-1369	342	10	with	with	ADP
eurjchem-1369	342	11	the	the	DET
eurjchem-1369	342	12	assigned	assign	VERB
eurjchem-1369	342	13	structures	structure	NOUN
eurjchem-1369	342	14	of	of	ADP
eurjchem-1369	342	15	compounds	compound	NOUN
eurjchem-1369	342	16	5	5	NUM
eurjchem-1369	342	17	and	and	CCONJ
eurjchem-1369	342	18	6a	6a	NOUN
eurjchem-1369	342	19	,	,	PUNCT
eurjchem-1369	342	20	b.	b.	PROPN
eurjchem-1369	343	1	the	the	DET
eurjchem-1369	343	2	mass	mass	PROPN
eurjchem-1369	343	3	spectrum	spectrum	NOUN
eurjchem-1369	343	4	showed	show	VERB
eurjchem-1369	343	5	molecular	molecular	ADJ
eurjchem-1369	343	6	ion	ion	NOUN
eurjchem-1369	343	7	peak	peak	NOUN
eurjchem-1369	343	8	at	at	ADP
eurjchem-1369	343	9	m	m	PROPN
eurjchem-1369	343	10	/	/	SYM
eurjchem-1369	343	11	z	z	PROPN
eurjchem-1369	343	12	277	277	NUM
eurjchem-1369	343	13	for	for	ADP
eurjchem-1369	343	14	compound	compound	NOUN
eurjchem-1369	343	15	5	5	NUM
eurjchem-1369	343	16	,	,	PUNCT
eurjchem-1369	343	17	at	at	ADP
eurjchem-1369	343	18	m	m	PROPN
eurjchem-1369	343	19	/	/	SYM
eurjchem-1369	343	20	z	z	NOUN
eurjchem-1369	343	21	279	279	NUM
eurjchem-1369	343	22	for	for	ADP
eurjchem-1369	343	23	compound	compound	NOUN
eurjchem-1369	343	24	6a	6a	NOUN
eurjchem-1369	343	25	and	and	CCONJ
eurjchem-1369	343	26	at	at	ADP
eurjchem-1369	343	27	m	m	PROPN
eurjchem-1369	343	28	/	/	SYM
eurjchem-1369	343	29	z	z	PROPN
eurjchem-1369	343	30	351	351	NUM
eurjchem-1369	343	31	for	for	ADP
eurjchem-1369	343	32	compound	compound	NOUN
eurjchem-1369	343	33	6b	6b	NOUN
eurjchem-1369	343	34	.	.	PUNCT
eurjchem-1369	343	35	13c	13c	NOUN
eurjchem-1369	343	36	nmr	nmr	NOUN
eurjchem-1369	343	37	of	of	ADP
eurjchem-1369	343	38	compounds	compound	NOUN
eurjchem-1369	343	39	6a	6a	NOUN
eurjchem-1369	343	40	and	and	CCONJ
eurjchem-1369	343	41	6b	6b	NOUN
eurjchem-1369	343	42	showed	show	VERB
eurjchem-1369	343	43	eleven	eleven	NUM
eurjchem-1369	343	44	and	and	CCONJ
eurjchem-1369	343	45	fourteen	fourteen	NUM
eurjchem-1369	343	46	different	different	ADJ
eurjchem-1369	343	47	signals	signal	NOUN
eurjchem-1369	343	48	for	for	ADP
eurjchem-1369	343	49	eleven	eleven	NUM
eurjchem-1369	343	50	and	and	CCONJ
eurjchem-1369	343	51	fourteen	fourteen	NUM
eurjchem-1369	343	52	different	different	ADJ
eurjchem-1369	343	53	carbons	carbon	NOUN
eurjchem-1369	343	54	,	,	PUNCT
eurjchem-1369	343	55	respectively	respectively	ADV
eurjchem-1369	343	56	(	(	PUNCT
eurjchem-1369	343	57	experimental	experimental	ADJ
eurjchem-1369	343	58	part	part	NOUN
eurjchem-1369	343	59	)	)	PUNCT
eurjchem-1369	343	60	.	.	PUNCT
eurjchem-1369	344	1	compound	compound	NOUN
eurjchem-1369	344	2	4a	4a	NOUN
eurjchem-1369	344	3	was	be	AUX
eurjchem-1369	344	4	reacted	react	VERB
eurjchem-1369	344	5	with	with	ADP
eurjchem-1369	344	6	2‐(3‐benzyloxy‐benzyl‐	2‐(3‐benzyloxy‐benzyl‐	NUM
eurjchem-1369	344	7	iden)malononitrile	iden)malononitrile	NOUN
eurjchem-1369	344	8	in	in	ADP
eurjchem-1369	344	9	pyridine	pyridine	NOUN
eurjchem-1369	344	10	to	to	PART
eurjchem-1369	344	11	give	give	VERB
eurjchem-1369	344	12	5‐amino‐7‐(3‐benzyl	5‐amino‐7‐(3‐benzyl	NUM
eurjchem-1369	344	13	oxy‐phenyl)‐6‐cyano‐2‐ureido‐4,7‐dihydropyrazolo[1	oxy‐phenyl)‐6‐cyano‐2‐ureido‐4,7‐dihydropyrazolo[1	NOUN
eurjchem-1369	344	14	,	,	PUNCT
eurjchem-1369	344	15	5‐a	5‐a	NUM
eurjchem-1369	344	16	]	]	PUNCT
eurjchem-1369	344	17	pyri‐	pyri‐	PROPN
eurjchem-1369	344	18	midine‐3‐carboxylic	midine‐3‐carboxylic	ADJ
eurjchem-1369	344	19	acid	acid	PROPN
eurjchem-1369	344	20	ethyl	ethyl	PROPN
eurjchem-1369	344	21	ester	ester	NOUN
eurjchem-1369	344	22	(	(	PUNCT
eurjchem-1369	344	23	7	7	NUM
eurjchem-1369	344	24	)	)	PUNCT
eurjchem-1369	344	25	,	,	PUNCT
eurjchem-1369	344	26	while	while	SCONJ
eurjchem-1369	344	27	the	the	DET
eurjchem-1369	344	28	other	other	ADJ
eurjchem-1369	344	29	isomer	isomer	NOUN
eurjchem-1369	344	30	8	8	NUM
eurjchem-1369	344	31	was	be	AUX
eurjchem-1369	344	32	not	not	PART
eurjchem-1369	344	33	traced	trace	VERB
eurjchem-1369	344	34	.	.	PUNCT
eurjchem-1369	345	1	the	the	DET
eurjchem-1369	345	2	chemical	chemical	ADJ
eurjchem-1369	345	3	structure	structure	NOUN
eurjchem-1369	345	4	of	of	ADP
eurjchem-1369	345	5	compound	compound	NOUN
eurjchem-1369	345	6	7	7	NUM
eurjchem-1369	345	7	was	be	AUX
eurjchem-1369	345	8	considered	consider	VERB
eurjchem-1369	345	9	more	more	ADV
eurjchem-1369	345	10	likely	likely	ADJ
eurjchem-1369	345	11	based	base	VERB
eurjchem-1369	345	12	on	on	ADP
eurjchem-1369	345	13	the	the	DET
eurjchem-1369	345	14	ring	ring	NOUN
eurjchem-1369	345	15	nitrogen	nitrogen	NOUN
eurjchem-1369	345	16	,	,	PUNCT
eurjchem-1369	345	17	which	which	PRON
eurjchem-1369	345	18	is	be	AUX
eurjchem-1369	345	19	the	the	DET
eurjchem-1369	345	20	most	most	ADV
eurjchem-1369	345	21	nucleophilic	nucleophilic	ADJ
eurjchem-1369	345	22	centre	centre	NOUN
eurjchem-1369	345	23	in	in	ADP
eurjchem-1369	345	24	the	the	DET
eurjchem-1369	345	25	molecule	molecule	NOUN
eurjchem-1369	345	26	.	.	PUNCT
eurjchem-1369	346	1	moreover	moreover	ADV
eurjchem-1369	346	2	,	,	PUNCT
eurjchem-1369	346	3	1h	1h	NUM
eurjchem-1369	346	4	nmr	nmr	NOUN
eurjchem-1369	346	5	showed	show	VERB
eurjchem-1369	346	6	an	an	DET
eurjchem-1369	346	7	amino	amino	NOUN
eurjchem-1369	346	8	function	function	NOUN
eurjchem-1369	346	9	at	at	ADP
eurjchem-1369	346	10	δ	δ	PROPN
eurjchem-1369	346	11	6.7	6.7	NUM
eurjchem-1369	346	12	ppm	ppm	NOUN
eurjchem-1369	346	13	and	and	CCONJ
eurjchem-1369	346	14	‐ch	‐ch	ADJ
eurjchem-1369	346	15	signal	signal	NOUN
eurjchem-1369	346	16	of	of	ADP
eurjchem-1369	346	17	c‐7	c‐7	PROPN
eurjchem-1369	346	18	at	at	ADP
eurjchem-1369	346	19	δ	δ	PROPN
eurjchem-1369	346	20	5.6	5.6	NUM
eurjchem-1369	346	21	ppm	ppm	NOUN
eurjchem-1369	346	22	.	.	PUNCT
eurjchem-1369	347	1	the	the	DET
eurjchem-1369	347	2	mass	mass	PROPN
eurjchem-1369	347	3	spectrum	spectrum	NOUN
eurjchem-1369	347	4	of	of	ADP
eurjchem-1369	347	5	compound	compound	NOUN
eurjchem-1369	347	6	7	7	NUM
eurjchem-1369	347	7	showed	show	VERB
eurjchem-1369	347	8	molecular	molecular	ADJ
eurjchem-1369	347	9	ion	ion	NOUN
eurjchem-1369	347	10	peak	peak	NOUN
eurjchem-1369	347	11	at	at	ADP
eurjchem-1369	347	12	m	m	PROPN
eurjchem-1369	347	13	/	/	SYM
eurjchem-1369	347	14	z	z	PROPN
eurjchem-1369	347	15	471	471	NUM
eurjchem-1369	347	16	corresponding	correspond	VERB
eurjchem-1369	347	17	to	to	ADP
eurjchem-1369	347	18	its	its	PRON
eurjchem-1369	347	19	molecular	molecular	ADJ
eurjchem-1369	347	20	formula	formula	NOUN
eurjchem-1369	347	21	(	(	PUNCT
eurjchem-1369	347	22	c24h21n7o4	c24h21n7o4	NOUN
eurjchem-1369	347	23	)	)	PUNCT
eurjchem-1369	347	24	.	.	PUNCT
eurjchem-1369	348	1	some	some	DET
eurjchem-1369	348	2	abbas‐temirek	abbas‐temirek	PROPN
eurjchem-1369	348	3	and	and	CCONJ
eurjchem-1369	348	4	abo‐bakr	abo‐bakr	ADJ
eurjchem-1369	348	5	/	/	SYM
eurjchem-1369	348	6	european	european	ADJ
eurjchem-1369	348	7	journal	journal	PROPN
eurjchem-1369	348	8	of	of	ADP
eurjchem-1369	348	9	chemistry	chemistry	NOUN
eurjchem-1369	348	10	7	7	NUM
eurjchem-1369	348	11	(	(	PUNCT
eurjchem-1369	348	12	1	1	NUM
eurjchem-1369	348	13	)	)	PUNCT
eurjchem-1369	348	14	(	(	PUNCT
eurjchem-1369	348	15	2016	2016	NUM
eurjchem-1369	348	16	)	)	PUNCT
eurjchem-1369	349	1	107‐114	107‐114	NUM
eurjchem-1369	349	2	113	113	NUM
eurjchem-1369	349	3	analogues	analogue	NOUN
eurjchem-1369	349	4	related	relate	VERB
eurjchem-1369	349	5	compounds	compound	NOUN
eurjchem-1369	349	6	reported	report	VERB
eurjchem-1369	349	7	in	in	ADP
eurjchem-1369	349	8	the	the	DET
eurjchem-1369	349	9	literature	literature	NOUN
eurjchem-1369	349	10	[	[	X
eurjchem-1369	349	11	21‐	21‐	NUM
eurjchem-1369	349	12	23	23	NUM
eurjchem-1369	349	13	]	]	PUNCT
eurjchem-1369	349	14	(	(	PUNCT
eurjchem-1369	349	15	scheme	scheme	NOUN
eurjchem-1369	349	16	2	2	NUM
eurjchem-1369	349	17	)	)	PUNCT
eurjchem-1369	349	18	.	.	PUNCT
eurjchem-1369	350	1	stirring	stir	VERB
eurjchem-1369	350	2	an	an	DET
eurjchem-1369	350	3	equimolar	equimolar	NOUN
eurjchem-1369	350	4	mixture	mixture	NOUN
eurjchem-1369	350	5	of	of	ADP
eurjchem-1369	350	6	compound	compound	NOUN
eurjchem-1369	350	7	4a	4a	NOUN
eurjchem-1369	350	8	and	and	CCONJ
eurjchem-1369	350	9	2‐	2‐	NUM
eurjchem-1369	350	10	cyano‐3,3‐bis(methylthio)acrylonitrile	cyano‐3,3‐bis(methylthio)acrylonitrile	NOUN
eurjchem-1369	351	1	[	[	X
eurjchem-1369	351	2	24	24	NUM
eurjchem-1369	351	3	]	]	PUNCT
eurjchem-1369	351	4	in	in	ADP
eurjchem-1369	351	5	dimethyl	dimethyl	NOUN
eurjchem-1369	351	6	form‐	form‐	ADJ
eurjchem-1369	351	7	amide	amide	NOUN
eurjchem-1369	351	8	containing	contain	VERB
eurjchem-1369	351	9	catalytic	catalytic	ADJ
eurjchem-1369	351	10	amount	amount	NOUN
eurjchem-1369	351	11	of	of	ADP
eurjchem-1369	351	12	potassium	potassium	NOUN
eurjchem-1369	351	13	carbonate	carbonate	NOUN
eurjchem-1369	351	14	at	at	ADP
eurjchem-1369	351	15	room	room	NOUN
eurjchem-1369	351	16	temperature	temperature	NOUN
eurjchem-1369	351	17	resulted	result	VERB
eurjchem-1369	351	18	in	in	ADP
eurjchem-1369	351	19	the	the	DET
eurjchem-1369	351	20	formation	formation	NOUN
eurjchem-1369	351	21	of	of	ADP
eurjchem-1369	351	22	the	the	DET
eurjchem-1369	351	23	corres‐	corres‐	NOUN
eurjchem-1369	351	24	ponding	ponde	VERB
eurjchem-1369	351	25	7‐amino‐6‐cyano‐5‐methylsulfanyl‐2‐ureido	7‐amino‐6‐cyano‐5‐methylsulfanyl‐2‐ureido	NUM
eurjchem-1369	351	26	pyrazolo	pyrazolo	NOUN
eurjchem-1369	352	1	[	[	X
eurjchem-1369	352	2	1,5‐a]pyrimidine‐3‐carboxylic	1,5‐a]pyrimidine‐3‐carboxylic	NUM
eurjchem-1369	352	3	acid	acid	NOUN
eurjchem-1369	352	4	ethyl	ethyl	NOUN
eurjchem-1369	352	5	ester	ester	NOUN
eurjchem-1369	352	6	(	(	PUNCT
eurjchem-1369	352	7	9	9	NUM
eurjchem-1369	352	8	)	)	PUNCT
eurjchem-1369	352	9	(	(	PUNCT
eurjchem-1369	352	10	scheme	scheme	NOUN
eurjchem-1369	352	11	2	2	NUM
eurjchem-1369	352	12	)	)	PUNCT
eurjchem-1369	352	13	.	.	PUNCT
eurjchem-1369	353	1	the	the	DET
eurjchem-1369	353	2	chemical	chemical	ADJ
eurjchem-1369	353	3	structure	structure	NOUN
eurjchem-1369	353	4	of	of	ADP
eurjchem-1369	353	5	compound	compound	NOUN
eurjchem-1369	353	6	9	9	NUM
eurjchem-1369	353	7	was	be	AUX
eurjchem-1369	353	8	assigned	assign	VERB
eurjchem-1369	353	9	on	on	ADP
eurjchem-1369	353	10	the	the	DET
eurjchem-1369	353	11	bases	basis	NOUN
eurjchem-1369	353	12	of	of	ADP
eurjchem-1369	353	13	its	its	PRON
eurjchem-1369	353	14	spectral	spectral	ADJ
eurjchem-1369	353	15	and	and	CCONJ
eurjchem-1369	353	16	elemental	elemental	ADJ
eurjchem-1369	353	17	data	datum	NOUN
eurjchem-1369	353	18	.	.	PUNCT
eurjchem-1369	354	1	ir	ir	PROPN
eurjchem-1369	354	2	spectrum	spectrum	NOUN
eurjchem-1369	354	3	of	of	ADP
eurjchem-1369	354	4	compound	compound	NOUN
eurjchem-1369	354	5	9	9	NUM
eurjchem-1369	354	6	showed	show	VERB
eurjchem-1369	354	7	absorption	absorption	NOUN
eurjchem-1369	354	8	bands	band	NOUN
eurjchem-1369	354	9	at	at	ADP
eurjchem-1369	354	10	3291‐3412	3291‐3412	NUM
eurjchem-1369	354	11	cm‐1	cm‐1	NOUN
eurjchem-1369	354	12	for	for	ADP
eurjchem-1369	354	13	2nh2	2nh2	NUM
eurjchem-1369	354	14	,	,	PUNCT
eurjchem-1369	354	15	3180	3180	NUM
eurjchem-1369	354	16	cm‐1	cm‐1	NOUN
eurjchem-1369	354	17	for	for	ADP
eurjchem-1369	354	18	nh	nh	PROPN
eurjchem-1369	354	19	,	,	PUNCT
eurjchem-1369	354	20	2215	2215	NUM
eurjchem-1369	354	21	cm‐1	cm‐1	NOUN
eurjchem-1369	354	22	for	for	ADP
eurjchem-1369	354	23	cn	cn	PROPN
eurjchem-1369	354	24	and	and	CCONJ
eurjchem-1369	354	25	at	at	ADP
eurjchem-1369	354	26	1682‐1719	1682‐1719	NUM
eurjchem-1369	354	27	cm‐1	cm‐1	NOUN
eurjchem-1369	354	28	for	for	ADP
eurjchem-1369	354	29	2c	2c	NUM
eurjchem-1369	354	30	=	=	NOUN
eurjchem-1369	354	31	o.	o.	NOUN
eurjchem-1369	354	32	the	the	DET
eurjchem-1369	354	33	1h	1h	NUM
eurjchem-1369	354	34	nmr	nmr	NOUN
eurjchem-1369	354	35	spectrum	spectrum	NOUN
eurjchem-1369	354	36	of	of	ADP
eurjchem-1369	354	37	compound	compound	NOUN
eurjchem-1369	354	38	9	9	NUM
eurjchem-1369	354	39	showed	show	VERB
eurjchem-1369	354	40	signals	signal	NOUN
eurjchem-1369	354	41	at	at	ADP
eurjchem-1369	354	42	δ	δ	PROPN
eurjchem-1369	354	43	1.23	1.23	NUM
eurjchem-1369	354	44	for	for	ADP
eurjchem-1369	354	45	ch3	ch3	PROPN
eurjchem-1369	354	46	,	,	PUNCT
eurjchem-1369	354	47	δ	δ	PROPN
eurjchem-1369	354	48	2.71	2.71	NUM
eurjchem-1369	354	49	for	for	ADP
eurjchem-1369	354	50	sch3	sch3	PROPN
eurjchem-1369	354	51	,	,	PUNCT
eurjchem-1369	354	52	δ	δ	PROPN
eurjchem-1369	354	53	4.2	4.2	NUM
eurjchem-1369	354	54	for	for	ADP
eurjchem-1369	354	55	ch2	ch2	PROPN
eurjchem-1369	354	56	,	,	PUNCT
eurjchem-1369	354	57	δ	δ	PROPN
eurjchem-1369	354	58	7.43	7.43	NUM
eurjchem-1369	354	59	,	,	PUNCT
eurjchem-1369	354	60	8.74	8.74	NUM
eurjchem-1369	354	61	for	for	ADP
eurjchem-1369	354	62	2nh2	2nh2	NUM
eurjchem-1369	354	63	and	and	CCONJ
eurjchem-1369	354	64	at	at	ADP
eurjchem-1369	354	65	δ	δ	PROPN
eurjchem-1369	354	66	8.62	8.62	NUM
eurjchem-1369	354	67	ppm	ppm	NOUN
eurjchem-1369	354	68	for	for	ADP
eurjchem-1369	354	69	nh	nh	PROPN
eurjchem-1369	354	70	.	.	PUNCT
eurjchem-1369	355	1	also	also	ADV
eurjchem-1369	355	2	,	,	PUNCT
eurjchem-1369	355	3	the	the	DET
eurjchem-1369	355	4	mass	mass	NOUN
eurjchem-1369	355	5	spectrum	spectrum	NOUN
eurjchem-1369	355	6	showed	show	VERB
eurjchem-1369	355	7	molecular	molecular	ADJ
eurjchem-1369	355	8	ion	ion	NOUN
eurjchem-1369	355	9	peak	peak	NOUN
eurjchem-1369	355	10	at	at	ADP
eurjchem-1369	355	11	m	m	PROPN
eurjchem-1369	355	12	/	/	SYM
eurjchem-1369	355	13	z	z	NOUN
eurjchem-1369	355	14	335	335	NUM
eurjchem-1369	355	15	corres‐	corres‐	NOUN
eurjchem-1369	355	16	ponding	ponde	VERB
eurjchem-1369	355	17	to	to	ADP
eurjchem-1369	355	18	its	its	PRON
eurjchem-1369	355	19	formula	formula	NOUN
eurjchem-1369	355	20	(	(	PUNCT
eurjchem-1369	355	21	c12h13n7o3s	c12h13n7o3s	NUM
eurjchem-1369	355	22	)	)	PUNCT
eurjchem-1369	355	23	.	.	PUNCT
eurjchem-1369	356	1	the	the	DET
eurjchem-1369	356	2	13c	13c	NUM
eurjchem-1369	356	3	nmr	nmr	NOUN
eurjchem-1369	356	4	spectrum	spectrum	NOUN
eurjchem-1369	356	5	of	of	ADP
eurjchem-1369	356	6	compound	compound	NOUN
eurjchem-1369	356	7	9	9	NUM
eurjchem-1369	356	8	showed	show	VERB
eurjchem-1369	356	9	twelve	twelve	NUM
eurjchem-1369	356	10	different	different	ADJ
eurjchem-1369	356	11	signals	signal	NOUN
eurjchem-1369	356	12	at	at	ADP
eurjchem-1369	356	13	δ	δ	PROPN
eurjchem-1369	356	14	14.39	14.39	NUM
eurjchem-1369	356	15	,	,	PUNCT
eurjchem-1369	356	16	16.32	16.32	NUM
eurjchem-1369	356	17	,	,	PUNCT
eurjchem-1369	356	18	59.74	59.74	NUM
eurjchem-1369	356	19	,	,	PUNCT
eurjchem-1369	356	20	84.23	84.23	NUM
eurjchem-1369	356	21	,	,	PUNCT
eurjchem-1369	356	22	84.5	84.5	NUM
eurjchem-1369	356	23	,	,	PUNCT
eurjchem-1369	356	24	114.12	114.12	NUM
eurjchem-1369	356	25	,	,	PUNCT
eurjchem-1369	356	26	142.94	142.94	NUM
eurjchem-1369	356	27	,	,	PUNCT
eurjchem-1369	356	28	153.15	153.15	NUM
eurjchem-1369	356	29	,	,	PUNCT
eurjchem-1369	356	30	153.99	153.99	NUM
eurjchem-1369	356	31	,	,	PUNCT
eurjchem-1369	356	32	154.46	154.46	NUM
eurjchem-1369	356	33	,	,	PUNCT
eurjchem-1369	356	34	157.40	157.40	NUM
eurjchem-1369	356	35	,	,	PUNCT
eurjchem-1369	356	36	163.62	163.62	NUM
eurjchem-1369	356	37	ppm	ppm	NOUN
eurjchem-1369	356	38	for	for	ADP
eurjchem-1369	356	39	twelve	twelve	NUM
eurjchem-1369	356	40	different	different	ADJ
eurjchem-1369	356	41	carbon	carbon	NOUN
eurjchem-1369	356	42	atoms	atom	NOUN
eurjchem-1369	356	43	,	,	PUNCT
eurjchem-1369	356	44	which	which	PRON
eurjchem-1369	356	45	adds	add	VERB
eurjchem-1369	356	46	additional	additional	ADJ
eurjchem-1369	356	47	confirmation	confirmation	NOUN
eurjchem-1369	356	48	for	for	ADP
eurjchem-1369	356	49	the	the	DET
eurjchem-1369	356	50	proposed	propose	VERB
eurjchem-1369	356	51	structure	structure	NOUN
eurjchem-1369	356	52	.	.	PUNCT
eurjchem-1369	357	1	in	in	ADP
eurjchem-1369	357	2	a	a	DET
eurjchem-1369	357	3	similar	similar	ADJ
eurjchem-1369	357	4	manner	manner	NOUN
eurjchem-1369	357	5	compound	compound	NOUN
eurjchem-1369	357	6	4a	4a	NOUN
eurjchem-1369	357	7	was	be	AUX
eurjchem-1369	357	8	reacted	react	VERB
eurjchem-1369	357	9	with	with	ADP
eurjchem-1369	357	10	3,3‐	3,3‐	NUM
eurjchem-1369	357	11	bis‐benzyl‐sulfanyl‐2‐cyano‐acrylic	bis‐benzyl‐sulfanyl‐2‐cyano‐acrylic	ADJ
eurjchem-1369	357	12	acid	acid	NOUN
eurjchem-1369	357	13	ethyl	ethyl	PROPN
eurjchem-1369	357	14	ester	ester	NOUN
eurjchem-1369	357	15	[	[	X
eurjchem-1369	357	16	24	24	NUM
eurjchem-1369	357	17	]	]	PUNCT
eurjchem-1369	357	18	,	,	PUNCT
eurjchem-1369	357	19	2‐	2‐	NUM
eurjchem-1369	357	20	cyano‐3‐ethoxy‐carbonylmethylsulfanyl‐3‐phenyl‐amino	cyano‐3‐ethoxy‐carbonylmethylsulfanyl‐3‐phenyl‐amino	PROPN
eurjchem-1369	357	21	acr‐	acr‐	PROPN
eurjchem-1369	357	22	ylic	ylic	PROPN
eurjchem-1369	357	23	acid	acid	PROPN
eurjchem-1369	357	24	ethyl	ethyl	PROPN
eurjchem-1369	357	25	ester	ester	NOUN
eurjchem-1369	357	26	and	and	CCONJ
eurjchem-1369	357	27	2‐cyano‐3‐methylsulfanyl‐3‐ureido‐	2‐cyano‐3‐methylsulfanyl‐3‐ureido‐	NUM
eurjchem-1369	357	28	acrylic	acrylic	NOUN
eurjchem-1369	357	29	acid	acid	NOUN
eurjchem-1369	357	30	ethyl	ethyl	PROPN
eurjchem-1369	357	31	ester	ester	NOUN
eurjchem-1369	358	1	[	[	X
eurjchem-1369	358	2	20	20	NUM
eurjchem-1369	358	3	]	]	PUNCT
eurjchem-1369	358	4	,	,	PUNCT
eurjchem-1369	358	5	to	to	PART
eurjchem-1369	358	6	give	give	VERB
eurjchem-1369	358	7	the	the	DET
eurjchem-1369	358	8	corresponding	correspond	VERB
eurjchem-1369	358	9	pyrazolo[1,5‐a]pyrimidine‐3‐carboxylic	pyrazolo[1,5‐a]pyrimidine‐3‐carboxylic	ADJ
eurjchem-1369	358	10	acid	acid	PROPN
eurjchem-1369	358	11	ethyl	ethyl	PROPN
eurjchem-1369	358	12	ester	ester	NOUN
eurjchem-1369	358	13	10a‐c	10a‐c	NOUN
eurjchem-1369	358	14	,	,	PUNCT
eurjchem-1369	358	15	respectively	respectively	ADV
eurjchem-1369	358	16	(	(	PUNCT
eurjchem-1369	358	17	scheme	scheme	NOUN
eurjchem-1369	358	18	3	3	NUM
eurjchem-1369	358	19	)	)	PUNCT
eurjchem-1369	358	20	.	.	PUNCT
eurjchem-1369	359	1	the	the	DET
eurjchem-1369	359	2	mass	mass	ADJ
eurjchem-1369	359	3	spectra	spectra	NOUN
eurjchem-1369	359	4	of	of	ADP
eurjchem-1369	359	5	compounds	compound	NOUN
eurjchem-1369	359	6	10a‐	10a‐	NUM
eurjchem-1369	359	7	c	c	NOUN
eurjchem-1369	359	8	showed	show	VERB
eurjchem-1369	359	9	molecular	molecular	ADJ
eurjchem-1369	359	10	ion	ion	NOUN
eurjchem-1369	359	11	peaks	peak	NOUN
eurjchem-1369	359	12	at	at	ADP
eurjchem-1369	359	13	m	m	PROPN
eurjchem-1369	359	14	/	/	SYM
eurjchem-1369	359	15	z	z	PROPN
eurjchem-1369	359	16	412	412	NUM
eurjchem-1369	359	17	for	for	ADP
eurjchem-1369	359	18	compound	compound	NOUN
eurjchem-1369	359	19	10a	10a	NOUN
eurjchem-1369	359	20	,	,	PUNCT
eurjchem-1369	359	21	at	at	ADP
eurjchem-1369	359	22	m	m	PROPN
eurjchem-1369	359	23	/	/	SYM
eurjchem-1369	359	24	z	z	PROPN
eurjchem-1369	359	25	381	381	NUM
eurjchem-1369	359	26	for	for	ADP
eurjchem-1369	359	27	compound	compound	NOUN
eurjchem-1369	359	28	10b	10b	NOUN
eurjchem-1369	359	29	and	and	CCONJ
eurjchem-1369	359	30	at	at	ADP
eurjchem-1369	359	31	m	m	PROPN
eurjchem-1369	359	32	/	/	SYM
eurjchem-1369	359	33	z	z	PROPN
eurjchem-1369	359	34	348	348	NUM
eurjchem-1369	359	35	for	for	ADP
eurjchem-1369	359	36	compound	compound	NOUN
eurjchem-1369	359	37	10c	10c	NOUN
eurjchem-1369	359	38	,	,	PUNCT
eurjchem-1369	359	39	led	lead	VERB
eurjchem-1369	359	40	to	to	ADP
eurjchem-1369	359	41	the	the	DET
eurjchem-1369	359	42	assignment	assignment	NOUN
eurjchem-1369	359	43	of	of	ADP
eurjchem-1369	359	44	their	their	PRON
eurjchem-1369	359	45	molecular	molecular	ADJ
eurjchem-1369	359	46	formulae	formulae	NOUN
eurjchem-1369	359	47	.	.	PUNCT
eurjchem-1369	360	1	analogously	analogously	ADV
eurjchem-1369	360	2	,	,	PUNCT
eurjchem-1369	360	3	condensation	condensation	NOUN
eurjchem-1369	360	4	of	of	ADP
eurjchem-1369	360	5	compound	compound	NOUN
eurjchem-1369	360	6	4a	4a	NOUN
eurjchem-1369	360	7	with	with	ADP
eurjchem-1369	360	8	ethyl‐2‐	ethyl‐2‐	NOUN
eurjchem-1369	360	9	cyano‐3,3‐bis(methylthio)acrylate	cyano‐3,3‐bis(methylthio)acrylate	NOUN
eurjchem-1369	360	10	and	and	CCONJ
eurjchem-1369	360	11	2‐cyano‐3,3‐bis‐methyl	2‐cyano‐3,3‐bis‐methyl	NUM
eurjchem-1369	360	12	sulfanyl‐acrylamide	sulfanyl‐acrylamide	ADV
eurjchem-1369	361	1	[	[	X
eurjchem-1369	361	2	25	25	NUM
eurjchem-1369	361	3	]	]	PUNCT
eurjchem-1369	361	4	,	,	PUNCT
eurjchem-1369	361	5	afforded	afford	VERB
eurjchem-1369	361	6	the	the	DET
eurjchem-1369	361	7	similar	similar	ADJ
eurjchem-1369	361	8	product	product	NOUN
eurjchem-1369	361	9	6‐	6‐	NOUN
eurjchem-1369	361	10	cyano‐5‐methyl‐sulfanyl‐7‐oxo‐2‐ureido‐4,7‐dihydropyrazolo	cyano‐5‐methyl‐sulfanyl‐7‐oxo‐2‐ureido‐4,7‐dihydropyrazolo	NOUN
eurjchem-1369	361	11	[	[	X
eurjchem-1369	361	12	1,5‐a]pyrimidine‐3‐carboxylic	1,5‐a]pyrimidine‐3‐carboxylic	NUM
eurjchem-1369	361	13	acid	acid	NOUN
eurjchem-1369	361	14	ethyl	ethyl	NOUN
eurjchem-1369	361	15	ester	ester	NOUN
eurjchem-1369	361	16	(	(	PUNCT
eurjchem-1369	361	17	11	11	NUM
eurjchem-1369	361	18	)	)	PUNCT
eurjchem-1369	361	19	.	.	PUNCT
eurjchem-1369	362	1	the	the	DET
eurjchem-1369	362	2	spectral	spectral	ADJ
eurjchem-1369	362	3	and	and	CCONJ
eurjchem-1369	362	4	analytical	analytical	ADJ
eurjchem-1369	362	5	data	datum	NOUN
eurjchem-1369	362	6	ruled	rule	VERB
eurjchem-1369	362	7	out	out	ADP
eurjchem-1369	362	8	the	the	DET
eurjchem-1369	362	9	alternative	alternative	ADJ
eurjchem-1369	362	10	products	product	NOUN
eurjchem-1369	362	11	12a	12a	NOUN
eurjchem-1369	362	12	and	and	CCONJ
eurjchem-1369	362	13	12b	12b	NOUN
eurjchem-1369	362	14	(	(	PUNCT
eurjchem-1369	362	15	scheme	scheme	NOUN
eurjchem-1369	362	16	3	3	NUM
eurjchem-1369	362	17	)	)	PUNCT
eurjchem-1369	362	18	,	,	PUNCT
eurjchem-1369	362	19	where	where	SCONJ
eurjchem-1369	362	20	the	the	DET
eurjchem-1369	362	21	1h	1h	NUM
eurjchem-1369	362	22	nmr	nmr	NOUN
eurjchem-1369	362	23	spectrum	spectrum	NOUN
eurjchem-1369	362	24	of	of	ADP
eurjchem-1369	362	25	compound	compound	NOUN
eurjchem-1369	362	26	11	11	NUM
eurjchem-1369	362	27	showed	show	VERB
eurjchem-1369	362	28	signals	signal	NOUN
eurjchem-1369	362	29	at	at	ADP
eurjchem-1369	362	30	δ	δ	PROPN
eurjchem-1369	362	31	2.50	2.50	NUM
eurjchem-1369	362	32	for	for	ADP
eurjchem-1369	362	33	ch3	ch3	PROPN
eurjchem-1369	362	34	,	,	PUNCT
eurjchem-1369	362	35	δ	δ	PROPN
eurjchem-1369	362	36	2.45	2.45	NUM
eurjchem-1369	362	37	for	for	ADP
eurjchem-1369	362	38	sme	sme	PROPN
eurjchem-1369	362	39	,	,	PUNCT
eurjchem-1369	362	40	δ	δ	PROPN
eurjchem-1369	362	41	3.88	3.88	NUM
eurjchem-1369	362	42	for	for	ADP
eurjchem-1369	362	43	pyrimidine‐nh	pyrimidine‐nh	NOUN
eurjchem-1369	362	44	,	,	PUNCT
eurjchem-1369	362	45	δ	δ	PROPN
eurjchem-1369	362	46	4.26	4.26	NUM
eurjchem-1369	362	47	for	for	ADP
eurjchem-1369	362	48	ch2	ch2	PROPN
eurjchem-1369	362	49	,	,	PUNCT
eurjchem-1369	362	50	δ	δ	PROPN
eurjchem-1369	362	51	7.17	7.17	NUM
eurjchem-1369	362	52	for	for	ADP
eurjchem-1369	362	53	nh2	nh2	PROPN
eurjchem-1369	362	54	and	and	CCONJ
eurjchem-1369	362	55	at	at	ADP
eurjchem-1369	362	56	δ	δ	PROPN
eurjchem-1369	362	57	8.32	8.32	NUM
eurjchem-1369	362	58	ppm	ppm	NOUN
eurjchem-1369	362	59	for	for	ADP
eurjchem-1369	362	60	nh	nh	NOUN
eurjchem-1369	362	61	,	,	PUNCT
eurjchem-1369	362	62	and	and	CCONJ
eurjchem-1369	362	63	the	the	DET
eurjchem-1369	362	64	mass	mass	NOUN
eurjchem-1369	362	65	spectrum	spectrum	NOUN
eurjchem-1369	362	66	showed	show	VERB
eurjchem-1369	362	67	molecular	molecular	ADJ
eurjchem-1369	362	68	ion	ion	NOUN
eurjchem-1369	362	69	peaks	peak	NOUN
eurjchem-1369	362	70	at	at	ADP
eurjchem-1369	362	71	m	m	PROPN
eurjchem-1369	362	72	/	/	SYM
eurjchem-1369	362	73	z	z	PROPN
eurjchem-1369	362	74	336	336	NUM
eurjchem-1369	362	75	.	.	PUNCT
eurjchem-1369	363	1	heating	heating	NOUN
eurjchem-1369	363	2	of	of	ADP
eurjchem-1369	363	3	compound	compound	NOUN
eurjchem-1369	363	4	4a	4a	NOUN
eurjchem-1369	363	5	with	with	ADP
eurjchem-1369	363	6	ethoxymethylene	ethoxymethylene	NOUN
eurjchem-1369	363	7	malononitrile	malononitrile	NOUN
eurjchem-1369	363	8	[	[	X
eurjchem-1369	363	9	26	26	NUM
eurjchem-1369	363	10	]	]	PUNCT
eurjchem-1369	363	11	or	or	CCONJ
eurjchem-1369	363	12	ethoxymethylene	ethoxymethylene	NOUN
eurjchem-1369	363	13	cyanoacetate	cyanoacetate	NOUN
eurjchem-1369	363	14	in	in	ADP
eurjchem-1369	363	15	acetic	acetic	ADJ
eurjchem-1369	363	16	acid	acid	NOUN
eurjchem-1369	363	17	afforded	afford	VERB
eurjchem-1369	363	18	the	the	DET
eurjchem-1369	363	19	pyrazolo	pyrazolo	ADJ
eurjchem-1369	363	20	pyrimidine	pyrimidine	NOUN
eurjchem-1369	363	21	derivatives	derivative	NOUN
eurjchem-1369	363	22	13a	13a	NOUN
eurjchem-1369	363	23	,	,	PUNCT
eurjchem-1369	363	24	b	b	NOUN
eurjchem-1369	363	25	,	,	PUNCT
eurjchem-1369	363	26	respectively	respectively	ADV
eurjchem-1369	363	27	(	(	PUNCT
eurjchem-1369	363	28	scheme	scheme	NOUN
eurjchem-1369	363	29	4	4	NUM
eurjchem-1369	363	30	)	)	PUNCT
eurjchem-1369	363	31	.	.	PUNCT
eurjchem-1369	364	1	the	the	DET
eurjchem-1369	364	2	chemical	chemical	NOUN
eurjchem-1369	364	3	structures	structure	NOUN
eurjchem-1369	364	4	of	of	ADP
eurjchem-1369	364	5	com‐	com‐	ADJ
eurjchem-1369	364	6	pounds	pound	NOUN
eurjchem-1369	364	7	13a	13a	NOUN
eurjchem-1369	364	8	and	and	CCONJ
eurjchem-1369	364	9	13b	13b	NOUN
eurjchem-1369	364	10	were	be	AUX
eurjchem-1369	364	11	proved	prove	VERB
eurjchem-1369	364	12	according	accord	VERB
eurjchem-1369	364	13	their	their	PRON
eurjchem-1369	364	14	elemental	elemental	ADJ
eurjchem-1369	364	15	and	and	CCONJ
eurjchem-1369	364	16	spectroscopic	spectroscopic	ADJ
eurjchem-1369	364	17	data	datum	NOUN
eurjchem-1369	364	18	,	,	PUNCT
eurjchem-1369	364	19	the	the	DET
eurjchem-1369	364	20	13c	13c	NOUN
eurjchem-1369	364	21	nmr	nmr	NOUN
eurjchem-1369	364	22	spectrum	spectrum	NOUN
eurjchem-1369	364	23	of	of	ADP
eurjchem-1369	364	24	compound	compound	NOUN
eurjchem-1369	364	25	13a	13a	PROPN
eurjchem-1369	364	26	showed	show	VERB
eurjchem-1369	364	27	the	the	DET
eurjchem-1369	364	28	presence	presence	NOUN
eurjchem-1369	364	29	of	of	ADP
eurjchem-1369	364	30	eleven	eleven	NUM
eurjchem-1369	364	31	different	different	ADJ
eurjchem-1369	364	32	signals	signal	NOUN
eurjchem-1369	364	33	corresponding	correspond	VERB
eurjchem-1369	364	34	to	to	ADP
eurjchem-1369	364	35	thier	thier	PRON
eurjchem-1369	364	36	different	different	ADJ
eurjchem-1369	364	37	carbons	carbon	NOUN
eurjchem-1369	364	38	at	at	ADP
eurjchem-1369	364	39	δ	δ	PROPN
eurjchem-1369	364	40	19.7	19.7	NUM
eurjchem-1369	364	41	(	(	PUNCT
eurjchem-1369	364	42	ch3	ch3	PROPN
eurjchem-1369	364	43	)	)	PUNCT
eurjchem-1369	364	44	,	,	PUNCT
eurjchem-1369	364	45	65.7	65.7	NUM
eurjchem-1369	364	46	(	(	PUNCT
eurjchem-1369	364	47	ch2	ch2	PROPN
eurjchem-1369	364	48	)	)	PUNCT
eurjchem-1369	364	49	,	,	PUNCT
eurjchem-1369	364	50	83.00	83.00	NUM
eurjchem-1369	364	51	(=	(=	NOUN
eurjchem-1369	364	52	c‐n	c‐n	NOUN
eurjchem-1369	364	53	)	)	PUNCT
eurjchem-1369	364	54	,	,	PUNCT
eurjchem-1369	364	55	93.36	93.36	NUM
eurjchem-1369	364	56	(	(	PUNCT
eurjchem-1369	364	57	n	n	CCONJ
eurjchem-1369	364	58	=	=	SYM
eurjchem-1369	364	59	c‐n	c‐n	NOUN
eurjchem-1369	364	60	)	)	PUNCT
eurjchem-1369	364	61	,	,	PUNCT
eurjchem-1369	364	62	120.9	120.9	NUM
eurjchem-1369	364	63	(	(	PUNCT
eurjchem-1369	364	64	n	n	CCONJ
eurjchem-1369	364	65	=	=	NOUN
eurjchem-1369	364	66	c‐nh2	c‐nh2	PROPN
eurjchem-1369	364	67	)	)	PUNCT
eurjchem-1369	364	68	,	,	PUNCT
eurjchem-1369	364	69	153.4	153.4	NUM
eurjchem-1369	364	70	(	(	PUNCT
eurjchem-1369	364	71	c	c	NOUN
eurjchem-1369	364	72	=	=	SYM
eurjchem-1369	364	73	c‐n	c‐n	NOUN
eurjchem-1369	364	74	)	)	PUNCT
eurjchem-1369	364	75	,	,	PUNCT
eurjchem-1369	364	76	154.3	154.3	NUM
eurjchem-1369	364	77	(=	(=	NOUN
eurjchem-1369	364	78	c‐cooet	c‐cooet	NUM
eurjchem-1369	364	79	)	)	PUNCT
eurjchem-1369	364	80	,	,	PUNCT
eurjchem-1369	364	81	158.7	158.7	NUM
eurjchem-1369	364	82	(=	(=	NOUN
eurjchem-1369	364	83	c‐cn	c‐cn	NOUN
eurjchem-1369	364	84	)	)	PUNCT
eurjchem-1369	364	85	,	,	PUNCT
eurjchem-1369	364	86	159.5	159.5	NUM
eurjchem-1369	364	87	(	(	PUNCT
eurjchem-1369	364	88	cn	cn	PROPN
eurjchem-1369	364	89	)	)	PUNCT
eurjchem-1369	364	90	,	,	PUNCT
eurjchem-1369	364	91	161.5	161.5	NUM
eurjchem-1369	364	92	(	(	PUNCT
eurjchem-1369	364	93	conh2	conh2	PROPN
eurjchem-1369	364	94	)	)	PUNCT
eurjchem-1369	364	95	and	and	CCONJ
eurjchem-1369	364	96	at	at	ADP
eurjchem-1369	364	97	δ	δ	PROPN
eurjchem-1369	364	98	169.5	169.5	NUM
eurjchem-1369	364	99	ppm	ppm	NOUN
eurjchem-1369	364	100	(	(	PUNCT
eurjchem-1369	364	101	cooet	cooet	NOUN
eurjchem-1369	364	102	)	)	PUNCT
eurjchem-1369	364	103	,	,	PUNCT
eurjchem-1369	364	104	which	which	PRON
eurjchem-1369	364	105	gives	give	VERB
eurjchem-1369	364	106	additional	additional	ADJ
eurjchem-1369	364	107	confirmation	confirmation	NOUN
eurjchem-1369	364	108	for	for	ADP
eurjchem-1369	364	109	the	the	DET
eurjchem-1369	364	110	proposed	propose	VERB
eurjchem-1369	364	111	structure	structure	NOUN
eurjchem-1369	364	112	.	.	PUNCT
eurjchem-1369	365	1	when	when	SCONJ
eurjchem-1369	365	2	compound	compound	NOUN
eurjchem-1369	365	3	4a	4a	NOUN
eurjchem-1369	365	4	was	be	AUX
eurjchem-1369	365	5	stirred	stir	VERB
eurjchem-1369	365	6	with	with	ADP
eurjchem-1369	365	7	n‐bis(methylthio	n‐bis(methylthio	NOUN
eurjchem-1369	365	8	)	)	PUNCT
eurjchem-1369	365	9	methylenecyanamide	methylenecyanamide	NOUN
eurjchem-1369	365	10	(	(	PUNCT
eurjchem-1369	365	11	1	1	X
eurjchem-1369	365	12	)	)	PUNCT
eurjchem-1369	365	13	in	in	ADP
eurjchem-1369	365	14	the	the	DET
eurjchem-1369	365	15	presence	presence	NOUN
eurjchem-1369	365	16	of	of	ADP
eurjchem-1369	365	17	potassium	potassium	NOUN
eurjchem-1369	365	18	carbonate	carbonate	NOUN
eurjchem-1369	365	19	in	in	ADP
eurjchem-1369	365	20	dimethylformamide	dimethylformamide	NOUN
eurjchem-1369	365	21	at	at	ADP
eurjchem-1369	365	22	room	room	NOUN
eurjchem-1369	365	23	temperature	temperature	NOUN
eurjchem-1369	365	24	,	,	PUNCT
eurjchem-1369	365	25	the	the	DET
eurjchem-1369	365	26	corresponding	correspond	VERB
eurjchem-1369	365	27	4‐amino‐2‐methylsulfanyl‐7‐ureido‐pyrazolo	4‐amino‐2‐methylsulfanyl‐7‐ureido‐pyrazolo	PROPN
eurjchem-1369	366	1	[	[	X
eurjchem-1369	366	2	1,5‐a][1,3,5]triazine‐8‐carboxylic	1,5‐a][1,3,5]triazine‐8‐carboxylic	NUM
eurjchem-1369	366	3	acid	acid	PROPN
eurjchem-1369	366	4	ethyl	ethyl	PROPN
eurjchem-1369	366	5	ester	ester	NOUN
eurjchem-1369	366	6	(	(	PUNCT
eurjchem-1369	366	7	14	14	NUM
eurjchem-1369	366	8	)	)	PUNCT
eurjchem-1369	366	9	was	be	AUX
eurjchem-1369	366	10	obtained	obtain	VERB
eurjchem-1369	366	11	.	.	PUNCT
eurjchem-1369	367	1	refluxing	refluxing	NOUN
eurjchem-1369	367	2	of	of	ADP
eurjchem-1369	367	3	equimolar	equimolar	ADJ
eurjchem-1369	367	4	quantities	quantity	NOUN
eurjchem-1369	367	5	of	of	ADP
eurjchem-1369	367	6	compound	compound	NOUN
eurjchem-1369	367	7	4a	4a	NOUN
eurjchem-1369	367	8	and	and	CCONJ
eurjchem-1369	367	9	salicylaldehyde	salicylaldehyde	NOUN
eurjchem-1369	367	10	in	in	ADP
eurjchem-1369	367	11	ethanol	ethanol	NOUN
eurjchem-1369	367	12	containing	contain	VERB
eurjchem-1369	367	13	catalytic	catalytic	ADJ
eurjchem-1369	367	14	amount	amount	NOUN
eurjchem-1369	367	15	of	of	ADP
eurjchem-1369	367	16	piperidine	piperidine	NOUN
eurjchem-1369	367	17	gave	give	VERB
eurjchem-1369	367	18	2‐ureido	2‐ureido	NUM
eurjchem-1369	367	19	pyrazolo[1,5‐a]quinazoline‐3‐car‐	pyrazolo[1,5‐a]quinazoline‐3‐car‐	ADP
eurjchem-1369	367	20	boxylic	boxylic	ADJ
eurjchem-1369	367	21	acid	acid	PROPN
eurjchem-1369	367	22	ethyl	ethyl	PROPN
eurjchem-1369	367	23	ester	ester	NOUN
eurjchem-1369	367	24	(	(	PUNCT
eurjchem-1369	367	25	15	15	NUM
eurjchem-1369	367	26	)	)	PUNCT
eurjchem-1369	367	27	.	.	PUNCT
eurjchem-1369	368	1	compound	compound	NOUN
eurjchem-1369	368	2	15	15	NUM
eurjchem-1369	368	3	was	be	AUX
eurjchem-1369	368	4	cyclized	cyclize	VERB
eurjchem-1369	368	5	into	into	ADP
eurjchem-1369	368	6	the	the	DET
eurjchem-1369	368	7	pyrazoloquinazoline	pyrazoloquinazoline	NOUN
eurjchem-1369	368	8	16	16	NUM
eurjchem-1369	368	9	by	by	ADP
eurjchem-1369	368	10	refluxing	refluxe	VERB
eurjchem-1369	368	11	in	in	ADP
eurjchem-1369	368	12	acetic	acetic	ADJ
eurjchem-1369	368	13	acid	acid	NOUN
eurjchem-1369	368	14	(	(	PUNCT
eurjchem-1369	368	15	scheme	scheme	NOUN
eurjchem-1369	368	16	4	4	NUM
eurjchem-1369	368	17	)	)	PUNCT
eurjchem-1369	368	18	.	.	PUNCT
eurjchem-1369	369	1	the	the	DET
eurjchem-1369	369	2	structures	structure	NOUN
eurjchem-1369	369	3	of	of	ADP
eurjchem-1369	369	4	compounds	compound	NOUN
eurjchem-1369	369	5	14	14	NUM
eurjchem-1369	369	6	,	,	PUNCT
eurjchem-1369	369	7	15	15	NUM
eurjchem-1369	369	8	and	and	CCONJ
eurjchem-1369	369	9	16	16	NUM
eurjchem-1369	369	10	were	be	AUX
eurjchem-1369	369	11	in	in	ADP
eurjchem-1369	369	12	agreement	agreement	NOUN
eurjchem-1369	369	13	with	with	ADP
eurjchem-1369	369	14	their	their	PRON
eurjchem-1369	369	15	spectral	spectral	ADJ
eurjchem-1369	369	16	data	datum	NOUN
eurjchem-1369	369	17	and	and	CCONJ
eurjchem-1369	369	18	elemental	elemental	ADJ
eurjchem-1369	369	19	analyses	analysis	NOUN
eurjchem-1369	369	20	.	.	PUNCT
eurjchem-1369	370	1	the	the	DET
eurjchem-1369	370	2	mass	mass	PROPN
eurjchem-1369	370	3	spectrum	spectrum	NOUN
eurjchem-1369	370	4	showed	show	VERB
eurjchem-1369	370	5	molecular	molecular	ADJ
eurjchem-1369	370	6	ion	ion	NOUN
eurjchem-1369	370	7	peak	peak	NOUN
eurjchem-1369	370	8	at	at	ADP
eurjchem-1369	370	9	m	m	PROPN
eurjchem-1369	370	10	/	/	SYM
eurjchem-1369	370	11	z	z	PROPN
eurjchem-1369	370	12	311	311	NUM
eurjchem-1369	370	13	for	for	ADP
eurjchem-1369	370	14	compound	compound	NOUN
eurjchem-1369	370	15	14	14	NUM
eurjchem-1369	370	16	,	,	PUNCT
eurjchem-1369	370	17	at	at	ADP
eurjchem-1369	370	18	m	m	PROPN
eurjchem-1369	370	19	/	/	SYM
eurjchem-1369	370	20	z	z	PROPN
eurjchem-1369	370	21	317	317	NUM
eurjchem-1369	370	22	for	for	ADP
eurjchem-1369	370	23	compound	compound	NOUN
eurjchem-1369	370	24	15	15	NUM
eurjchem-1369	370	25	and	and	CCONJ
eurjchem-1369	370	26	at	at	ADP
eurjchem-1369	370	27	m	m	PROPN
eurjchem-1369	370	28	/	/	SYM
eurjchem-1369	370	29	z	z	PROPN
eurjchem-1369	370	30	299	299	NUM
eurjchem-1369	370	31	for	for	ADP
eurjchem-1369	370	32	compound	compound	NOUN
eurjchem-1369	370	33	16	16	NUM
eurjchem-1369	370	34	,	,	PUNCT
eurjchem-1369	370	35	which	which	PRON
eurjchem-1369	370	36	were	be	AUX
eurjchem-1369	370	37	in	in	ADP
eurjchem-1369	370	38	consistent	consistent	ADJ
eurjchem-1369	370	39	with	with	ADP
eurjchem-1369	370	40	their	their	PRON
eurjchem-1369	370	41	corres‐	corres‐	NOUN
eurjchem-1369	370	42	ponding	ponde	VERB
eurjchem-1369	370	43	formulae	formulae	NOUN
eurjchem-1369	370	44	(	(	PUNCT
eurjchem-1369	370	45	experimental	experimental	ADJ
eurjchem-1369	370	46	part	part	NOUN
eurjchem-1369	370	47	)	)	PUNCT
eurjchem-1369	370	48	.	.	PUNCT
eurjchem-1369	371	1	treatment	treatment	NOUN
eurjchem-1369	371	2	of	of	ADP
eurjchem-1369	371	3	compound	compound	NOUN
eurjchem-1369	371	4	4a	4a	NOUN
eurjchem-1369	371	5	with	with	ADP
eurjchem-1369	371	6	nitrous	nitrous	ADJ
eurjchem-1369	371	7	acid	acid	NOUN
eurjchem-1369	371	8	in	in	ADP
eurjchem-1369	371	9	presence	presence	NOUN
eurjchem-1369	371	10	of	of	ADP
eurjchem-1369	371	11	concentrated	concentrated	ADJ
eurjchem-1369	371	12	hydrochloric	hydrochloric	ADJ
eurjchem-1369	371	13	acid	acid	NOUN
eurjchem-1369	371	14	/	/	SYM
eurjchem-1369	371	15	acetic	acetic	ADJ
eurjchem-1369	371	16	acid	acid	NOUN
eurjchem-1369	371	17	mixture	mixture	NOUN
eurjchem-1369	371	18	gave	give	VERB
eurjchem-1369	371	19	the	the	DET
eurjchem-1369	371	20	corresponding	corresponding	ADJ
eurjchem-1369	371	21	diazonium	diazonium	NOUN
eurjchem-1369	371	22	salt	salt	NOUN
eurjchem-1369	371	23	17	17	NUM
eurjchem-1369	372	1	[	[	X
eurjchem-1369	372	2	20	20	NUM
eurjchem-1369	372	3	]	]	PUNCT
eurjchem-1369	372	4	,	,	PUNCT
eurjchem-1369	373	1	which	which	PRON
eurjchem-1369	373	2	could	could	AUX
eurjchem-1369	373	3	not	not	PART
eurjchem-1369	373	4	be	be	AUX
eurjchem-1369	373	5	isolated	isolate	VERB
eurjchem-1369	373	6	in	in	ADP
eurjchem-1369	373	7	pure	pure	ADJ
eurjchem-1369	373	8	status	status	NOUN
eurjchem-1369	373	9	but	but	CCONJ
eurjchem-1369	373	10	its	its	PRON
eurjchem-1369	373	11	formation	formation	NOUN
eurjchem-1369	373	12	was	be	AUX
eurjchem-1369	373	13	indicated	indicate	VERB
eurjchem-1369	373	14	via	via	ADP
eurjchem-1369	373	15	coupling	couple	VERB
eurjchem-1369	373	16	with	with	ADP
eurjchem-1369	373	17	some	some	DET
eurjchem-1369	373	18	phenols	phenol	NOUN
eurjchem-1369	373	19	and	and	CCONJ
eurjchem-1369	373	20	active	active	ADJ
eurjchem-1369	373	21	methylene	methylene	NOUN
eurjchem-1369	373	22	reagents	reagent	NOUN
eurjchem-1369	373	23	.	.	PUNCT
eurjchem-1369	374	1	so	so	ADV
eurjchem-1369	374	2	,	,	PUNCT
eurjchem-1369	374	3	coupling	coupling	NOUN
eurjchem-1369	374	4	of	of	ADP
eurjchem-1369	374	5	the	the	DET
eurjchem-1369	374	6	diazonium	diazonium	NOUN
eurjchem-1369	374	7	salt	salt	NOUN
eurjchem-1369	374	8	17	17	NUM
eurjchem-1369	374	9	with	with	ADP
eurjchem-1369	374	10	2‐naphthol	2‐naphthol	NUM
eurjchem-1369	374	11	and	and	CCONJ
eurjchem-1369	374	12	resorcinol	resorcinol	NOUN
eurjchem-1369	374	13	afforded	afford	VERB
eurjchem-1369	374	14	the	the	DET
eurjchem-1369	374	15	corresponding	correspond	VERB
eurjchem-1369	374	16	arylazo	arylazo	ADV
eurjchem-1369	374	17	derivatives	derivative	NOUN
eurjchem-1369	374	18	18	18	NUM
eurjchem-1369	374	19	and	and	CCONJ
eurjchem-1369	374	20	20	20	NUM
eurjchem-1369	374	21	,	,	PUNCT
eurjchem-1369	374	22	respectively	respectively	ADV
eurjchem-1369	374	23	.	.	PUNCT
eurjchem-1369	375	1	cyclic	cyclic	ADJ
eurjchem-1369	375	2	condensation	condensation	NOUN
eurjchem-1369	375	3	of	of	ADP
eurjchem-1369	375	4	compound	compound	NOUN
eurjchem-1369	375	5	18	18	NUM
eurjchem-1369	375	6	and	and	CCONJ
eurjchem-1369	375	7	20	20	NUM
eurjchem-1369	375	8	in	in	ADP
eurjchem-1369	375	9	refluxing	refluxing	NOUN
eurjchem-1369	375	10	acetic	acetic	ADJ
eurjchem-1369	375	11	acid	acid	NOUN
eurjchem-1369	375	12	gave	give	VERB
eurjchem-1369	375	13	the	the	DET
eurjchem-1369	375	14	corresponding	correspond	VERB
eurjchem-1369	375	15	19	19	NUM
eurjchem-1369	375	16	and	and	CCONJ
eurjchem-1369	375	17	21	21	NUM
eurjchem-1369	375	18	,	,	PUNCT
eurjchem-1369	375	19	respectively	respectively	ADV
eurjchem-1369	375	20	(	(	PUNCT
eurjchem-1369	375	21	scheme	scheme	NOUN
eurjchem-1369	375	22	5	5	NUM
eurjchem-1369	375	23	)	)	PUNCT
eurjchem-1369	375	24	.	.	PUNCT
eurjchem-1369	376	1	this	this	DET
eurjchem-1369	376	2	result	result	NOUN
eurjchem-1369	376	3	is	be	AUX
eurjchem-1369	376	4	in	in	ADP
eurjchem-1369	376	5	contrast	contrast	NOUN
eurjchem-1369	376	6	with	with	ADP
eurjchem-1369	376	7	the	the	DET
eurjchem-1369	376	8	reported	report	VERB
eurjchem-1369	376	9	direct	direct	ADJ
eurjchem-1369	376	10	formation	formation	NOUN
eurjchem-1369	376	11	of	of	ADP
eurjchem-1369	376	12	cyclic	cyclic	ADJ
eurjchem-1369	376	13	pyrazolo[1,5‐c][1,2,4	pyrazolo[1,5‐c][1,2,4	NOUN
eurjchem-1369	376	14	]	]	PUNCT
eurjchem-1369	376	15	triazine	triazine	NOUN
eurjchem-1369	376	16	on	on	ADP
eurjchem-1369	376	17	coupling	couple	VERB
eurjchem-1369	376	18	diazotized	diazotize	VERB
eurjchem-1369	376	19	aminopyrazoles	aminopyrazole	NOUN
eurjchem-1369	376	20	with	with	ADP
eurjchem-1369	376	21	naphthols	naphthol	NOUN
eurjchem-1369	376	22	[	[	X
eurjchem-1369	376	23	27	27	NUM
eurjchem-1369	376	24	]	]	PUNCT
eurjchem-1369	376	25	.	.	PUNCT
eurjchem-1369	377	1	the	the	DET
eurjchem-1369	377	2	elemental	elemental	ADJ
eurjchem-1369	377	3	analyses	analysis	NOUN
eurjchem-1369	377	4	and	and	CCONJ
eurjchem-1369	377	5	spectroscopic	spectroscopic	ADJ
eurjchem-1369	377	6	data	datum	NOUN
eurjchem-1369	377	7	are	be	AUX
eurjchem-1369	377	8	in	in	ADP
eurjchem-1369	377	9	consistent	consistent	ADJ
eurjchem-1369	377	10	with	with	ADP
eurjchem-1369	377	11	the	the	DET
eurjchem-1369	377	12	assigned	assign	VERB
eurjchem-1369	377	13	structures	structure	NOUN
eurjchem-1369	377	14	of	of	ADP
eurjchem-1369	377	15	compounds	compound	NOUN
eurjchem-1369	377	16	18	18	NUM
eurjchem-1369	377	17	,	,	PUNCT
eurjchem-1369	377	18	19	19	NUM
eurjchem-1369	377	19	,	,	PUNCT
eurjchem-1369	377	20	20	20	NUM
eurjchem-1369	377	21	and	and	CCONJ
eurjchem-1369	377	22	21	21	NUM
eurjchem-1369	377	23	.	.	PUNCT
eurjchem-1369	378	1	the	the	DET
eurjchem-1369	378	2	1h	1h	NUM
eurjchem-1369	378	3	nmr	nmr	NOUN
eurjchem-1369	378	4	of	of	ADP
eurjchem-1369	378	5	compounds	compound	NOUN
eurjchem-1369	378	6	18	18	NUM
eurjchem-1369	378	7	and	and	CCONJ
eurjchem-1369	378	8	20	20	NUM
eurjchem-1369	378	9	showed	show	VERB
eurjchem-1369	378	10	presence	presence	NOUN
eurjchem-1369	378	11	of	of	ADP
eurjchem-1369	378	12	the	the	DET
eurjchem-1369	378	13	phenolic	phenolic	NOUN
eurjchem-1369	378	14	(	(	PUNCT
eurjchem-1369	378	15	oh	oh	INTJ
eurjchem-1369	378	16	)	)	PUNCT
eurjchem-1369	378	17	at	at	ADP
eurjchem-1369	378	18	δ	δ	PROPN
eurjchem-1369	378	19	10.8	10.8	NUM
eurjchem-1369	378	20	ppm	ppm	NOUN
eurjchem-1369	378	21	and	and	CCONJ
eurjchem-1369	378	22	δ	δ	PROPN
eurjchem-1369	378	23	11.2	11.2	NUM
eurjchem-1369	378	24	ppm	ppm	NOUN
eurjchem-1369	378	25	as	as	ADP
eurjchem-1369	378	26	broad	broad	ADJ
eurjchem-1369	378	27	peaks	peak	NOUN
eurjchem-1369	378	28	,	,	PUNCT
eurjchem-1369	378	29	respectively	respectively	ADV
eurjchem-1369	378	30	,	,	PUNCT
eurjchem-1369	378	31	which	which	PRON
eurjchem-1369	378	32	it	it	PRON
eurjchem-1369	378	33	disappeared	disappear	VERB
eurjchem-1369	378	34	in	in	ADP
eurjchem-1369	378	35	compound	compound	NOUN
eurjchem-1369	378	36	19	19	NUM
eurjchem-1369	378	37	.	.	PUNCT
eurjchem-1369	378	38	mass	mass	PROPN
eurjchem-1369	378	39	spectra	spectra	NOUN
eurjchem-1369	378	40	of	of	ADP
eurjchem-1369	378	41	compounds	compound	NOUN
eurjchem-1369	378	42	18	18	NUM
eurjchem-1369	378	43	,	,	PUNCT
eurjchem-1369	378	44	19	19	NUM
eurjchem-1369	378	45	,	,	PUNCT
eurjchem-1369	378	46	20	20	NUM
eurjchem-1369	378	47	and	and	CCONJ
eurjchem-1369	378	48	21	21	NUM
eurjchem-1369	378	49	showed	show	VERB
eurjchem-1369	378	50	ion	ion	NOUN
eurjchem-1369	378	51	peaks	peak	NOUN
eurjchem-1369	378	52	at	at	ADP
eurjchem-1369	378	53	m	m	PROPN
eurjchem-1369	378	54	/	/	SYM
eurjchem-1369	378	55	z	z	PROPN
eurjchem-1369	378	56	368	368	NUM
eurjchem-1369	378	57	,	,	PUNCT
eurjchem-1369	378	58	350	350	NUM
eurjchem-1369	378	59	,	,	PUNCT
eurjchem-1369	378	60	334	334	NUM
eurjchem-1369	378	61	and	and	CCONJ
eurjchem-1369	378	62	at	at	ADP
eurjchem-1369	378	63	m	m	PROPN
eurjchem-1369	378	64	/	/	SYM
eurjchem-1369	378	65	z	z	PROPN
eurjchem-1369	378	66	316	316	NUM
eurjchem-1369	378	67	,	,	PUNCT
eurjchem-1369	378	68	respectively	respectively	ADV
eurjchem-1369	378	69	,	,	PUNCT
eurjchem-1369	378	70	which	which	PRON
eurjchem-1369	378	71	were	be	AUX
eurjchem-1369	378	72	in	in	ADP
eurjchem-1369	378	73	agreement	agreement	NOUN
eurjchem-1369	378	74	with	with	ADP
eurjchem-1369	378	75	assigned	assign	VERB
eurjchem-1369	378	76	structures	structure	NOUN
eurjchem-1369	378	77	.	.	PUNCT
eurjchem-1369	379	1	in	in	ADP
eurjchem-1369	379	2	contrast	contrast	NOUN
eurjchem-1369	379	3	to	to	ADP
eurjchem-1369	379	4	the	the	DET
eurjchem-1369	379	5	previous	previous	ADJ
eurjchem-1369	379	6	results	result	NOUN
eurjchem-1369	379	7	,	,	PUNCT
eurjchem-1369	379	8	the	the	DET
eurjchem-1369	379	9	salt	salt	NOUN
eurjchem-1369	379	10	17	17	NUM
eurjchem-1369	379	11	was	be	AUX
eurjchem-1369	379	12	coupled	couple	VERB
eurjchem-1369	379	13	with	with	ADP
eurjchem-1369	379	14	ethyl	ethyl	PROPN
eurjchem-1369	379	15	cyanoacetate	cyanoacetate	NOUN
eurjchem-1369	379	16	to	to	PART
eurjchem-1369	379	17	yield	yield	VERB
eurjchem-1369	379	18	compound	compound	NOUN
eurjchem-1369	379	19	22a	22a	NOUN
eurjchem-1369	379	20	of	of	ADP
eurjchem-1369	379	21	the	the	DET
eurjchem-1369	379	22	molecular	molecular	ADJ
eurjchem-1369	379	23	formula	formula	NOUN
eurjchem-1369	379	24	c10h10n8o3	c10h10n8o3	PROPN
eurjchem-1369	379	25	(	(	PUNCT
eurjchem-1369	379	26	m	m	PROPN
eurjchem-1369	379	27	/	/	SYM
eurjchem-1369	379	28	z	z	PROPN
eurjchem-1369	379	29	290	290	NUM
eurjchem-1369	379	30	)	)	PUNCT
eurjchem-1369	379	31	,	,	PUNCT
eurjchem-1369	379	32	which	which	PRON
eurjchem-1369	379	33	was	be	AUX
eurjchem-1369	379	34	formulated	formulate	VERB
eurjchem-1369	379	35	as	as	ADP
eurjchem-1369	379	36	the	the	DET
eurjchem-1369	379	37	pyrazolo[1,5‐c][1,3,5]triazine	pyrazolo[1,5‐c][1,3,5]triazine	PROPN
eurjchem-1369	379	38	based	base	VERB
eurjchem-1369	379	39	on	on	ADP
eurjchem-1369	379	40	its	its	PRON
eurjchem-1369	379	41	spectral	spectral	ADJ
eurjchem-1369	379	42	data	datum	NOUN
eurjchem-1369	379	43	.	.	PUNCT
eurjchem-1369	380	1	thus	thus	ADV
eurjchem-1369	380	2	,	,	PUNCT
eurjchem-1369	380	3	the	the	DET
eurjchem-1369	380	4	ft‐ir	ft‐ir	NOUN
eurjchem-1369	380	5	spectrum	spectrum	NOUN
eurjchem-1369	380	6	showed	show	VERB
eurjchem-1369	380	7	the	the	DET
eurjchem-1369	380	8	presence	presence	NOUN
eurjchem-1369	380	9	of	of	ADP
eurjchem-1369	380	10	an	an	DET
eurjchem-1369	380	11	amino	amino	NOUN
eurjchem-1369	380	12	function	function	NOUN
eurjchem-1369	380	13	at	at	ADP
eurjchem-1369	380	14	3320	3320	NUM
eurjchem-1369	380	15	cm‐1	cm‐1	NOUN
eurjchem-1369	380	16	,	,	PUNCT
eurjchem-1369	380	17	and	and	CCONJ
eurjchem-1369	380	18	an	an	DET
eurjchem-1369	380	19	ester	ester	NOUN
eurjchem-1369	380	20	carbonyl	carbonyl	NOUN
eurjchem-1369	380	21	at	at	ADP
eurjchem-1369	380	22	1720	1720	NUM
eurjchem-1369	380	23	cm‐1	cm‐1	NOUN
eurjchem-1369	380	24	.	.	PUNCT
eurjchem-1369	381	1	the	the	DET
eurjchem-1369	381	2	1h	1h	NUM
eurjchem-1369	381	3	nmr	nmr	NOUN
eurjchem-1369	381	4	spectrum	spectrum	NOUN
eurjchem-1369	381	5	showed	show	VERB
eurjchem-1369	381	6	an	an	DET
eurjchem-1369	381	7	absorption	absorption	NOUN
eurjchem-1369	381	8	band	band	NOUN
eurjchem-1369	381	9	at	at	ADP
eurjchem-1369	381	10	δ	δ	PROPN
eurjchem-1369	381	11	8.8	8.8	NUM
eurjchem-1369	381	12	ppm	ppm	NOUN
eurjchem-1369	381	13	that	that	SCONJ
eurjchem-1369	381	14	it	it	PRON
eurjchem-1369	381	15	was	be	AUX
eurjchem-1369	381	16	integrated	integrate	VERB
eurjchem-1369	381	17	for	for	ADP
eurjchem-1369	381	18	two	two	NUM
eurjchem-1369	381	19	protons	proton	NOUN
eurjchem-1369	381	20	and	and	CCONJ
eurjchem-1369	381	21	was	be	AUX
eurjchem-1369	381	22	assigned	assign	VERB
eurjchem-1369	381	23	for	for	ADP
eurjchem-1369	381	24	the	the	DET
eurjchem-1369	381	25	amino	amino	NOUN
eurjchem-1369	381	26	group	group	NOUN
eurjchem-1369	381	27	.	.	PUNCT
eurjchem-1369	382	1	the	the	DET
eurjchem-1369	382	2	downfield	downfield	ADJ
eurjchem-1369	382	3	shift	shift	NOUN
eurjchem-1369	382	4	of	of	ADP
eurjchem-1369	382	5	this	this	DET
eurjchem-1369	382	6	amino	amino	NOUN
eurjchem-1369	382	7	function	function	NOUN
eurjchem-1369	382	8	could	could	AUX
eurjchem-1369	382	9	be	be	AUX
eurjchem-1369	382	10	explained	explain	VERB
eurjchem-1369	382	11	by	by	ADP
eurjchem-1369	382	12	the	the	DET
eurjchem-1369	382	13	anisotropic	anisotropic	NOUN
eurjchem-1369	382	14	effect	effect	NOUN
eurjchem-1369	382	15	of	of	ADP
eurjchem-1369	382	16	the	the	DET
eurjchem-1369	382	17	ring	ring	NOUN
eurjchem-1369	382	18	nitrogen	nitrogen	NOUN
eurjchem-1369	382	19	.	.	PUNCT
eurjchem-1369	383	1	in	in	ADP
eurjchem-1369	383	2	addition	addition	NOUN
eurjchem-1369	383	3	,	,	PUNCT
eurjchem-1369	383	4	1h	1h	NUM
eurjchem-1369	383	5	nmr	nmr	NOUN
eurjchem-1369	383	6	showed	show	VERB
eurjchem-1369	383	7	two	two	NUM
eurjchem-1369	383	8	ethyl	ethyl	PROPN
eurjchem-1369	383	9	ester	ester	NOUN
eurjchem-1369	383	10	groups	group	NOUN
eurjchem-1369	383	11	.	.	PUNCT
eurjchem-1369	384	1	in	in	ADP
eurjchem-1369	384	2	the	the	DET
eurjchem-1369	384	3	same	same	ADJ
eurjchem-1369	384	4	way	way	NOUN
eurjchem-1369	384	5	,	,	PUNCT
eurjchem-1369	384	6	compound	compound	NOUN
eurjchem-1369	384	7	17	17	NUM
eurjchem-1369	384	8	was	be	AUX
eurjchem-1369	384	9	coupled	couple	VERB
eurjchem-1369	384	10	with	with	ADP
eurjchem-1369	384	11	malononitrile	malononitrile	NOUN
eurjchem-1369	384	12	to	to	PART
eurjchem-1369	384	13	afford	afford	VERB
eurjchem-1369	384	14	the	the	DET
eurjchem-1369	384	15	corresponding	corresponding	ADJ
eurjchem-1369	384	16	pyrazolo[1,5‐c	pyrazolo[1,5‐c	PROPN
eurjchem-1369	384	17	]	]	X
eurjchem-1369	385	1	[	[	X
eurjchem-1369	385	2	1,3,5]triazine	1,3,5]triazine	NUM
eurjchem-1369	385	3	,	,	PUNCT
eurjchem-1369	385	4	22b	22b	NUM
eurjchem-1369	385	5	(	(	PUNCT
eurjchem-1369	385	6	scheme	scheme	NOUN
eurjchem-1369	385	7	5	5	NUM
eurjchem-1369	385	8	)	)	PUNCT
eurjchem-1369	385	9	.	.	PUNCT
eurjchem-1369	386	1	the	the	DET
eurjchem-1369	386	2	ft‐ir	ft‐ir	NOUN
eurjchem-1369	386	3	spectrum	spectrum	NOUN
eurjchem-1369	386	4	of	of	ADP
eurjchem-1369	386	5	compound	compound	NOUN
eurjchem-1369	386	6	22b	22b	NOUN
eurjchem-1369	386	7	showed	show	VERB
eurjchem-1369	386	8	the	the	DET
eurjchem-1369	386	9	presence	presence	NOUN
eurjchem-1369	386	10	of	of	ADP
eurjchem-1369	386	11	an	an	DET
eurjchem-1369	386	12	amino	amino	NOUN
eurjchem-1369	386	13	function	function	NOUN
eurjchem-1369	386	14	at	at	ADP
eurjchem-1369	386	15	3385‐3326	3385‐3326	NUM
eurjchem-1369	386	16	cm‐1	cm‐1	NOUN
eurjchem-1369	386	17	,	,	PUNCT
eurjchem-1369	386	18	and	and	CCONJ
eurjchem-1369	386	19	cyno	cyno	ADJ
eurjchem-1369	386	20	function	function	NOUN
eurjchem-1369	386	21	at	at	ADP
eurjchem-1369	386	22	2215	2215	NUM
eurjchem-1369	386	23	cm‐1	cm‐1	NOUN
eurjchem-1369	386	24	and	and	CCONJ
eurjchem-1369	386	25	the	the	DET
eurjchem-1369	386	26	1h	1h	NUM
eurjchem-1369	386	27	nmr	nmr	NOUN
eurjchem-1369	386	28	spectrum	spectrum	NOUN
eurjchem-1369	386	29	showed	show	VERB
eurjchem-1369	386	30	absorption	absorption	NOUN
eurjchem-1369	386	31	bands	band	NOUN
eurjchem-1369	386	32	at	at	ADP
eurjchem-1369	386	33	δ	δ	PROPN
eurjchem-1369	386	34	8.38	8.38	NUM
eurjchem-1369	386	35	ppm	ppm	NOUN
eurjchem-1369	386	36	for	for	ADP
eurjchem-1369	386	37	nh	nh	PROPN
eurjchem-1369	386	38	,	,	PUNCT
eurjchem-1369	386	39	δ	δ	PROPN
eurjchem-1369	386	40	7.37	7.37	NUM
eurjchem-1369	386	41	and	and	CCONJ
eurjchem-1369	386	42	6.58	6.58	NUM
eurjchem-1369	386	43	for	for	ADP
eurjchem-1369	386	44	two	two	NUM
eurjchem-1369	386	45	nh2	nh2	NOUN
eurjchem-1369	386	46	and	and	CCONJ
eurjchem-1369	386	47	at	at	ADP
eurjchem-1369	386	48	δ	δ	PROPN
eurjchem-1369	386	49	1.15	1.15	NUM
eurjchem-1369	386	50	and	and	CCONJ
eurjchem-1369	386	51	4.20	4.20	NUM
eurjchem-1369	386	52	ppm	ppm	NOUN
eurjchem-1369	386	53	corresponding	correspond	VERB
eurjchem-1369	386	54	to	to	ADP
eurjchem-1369	386	55	the	the	DET
eurjchem-1369	386	56	ethyl	ethyl	PROPN
eurjchem-1369	386	57	ester	ester	NOUN
eurjchem-1369	386	58	group	group	NOUN
eurjchem-1369	386	59	,	,	PUNCT
eurjchem-1369	386	60	which	which	PRON
eurjchem-1369	386	61	were	be	AUX
eurjchem-1369	386	62	in	in	ADP
eurjchem-1369	386	63	agreement	agreement	NOUN
eurjchem-1369	386	64	with	with	ADP
eurjchem-1369	386	65	its	its	PRON
eurjchem-1369	386	66	structure	structure	NOUN
eurjchem-1369	386	67	.	.	PUNCT
eurjchem-1369	387	1	4	4	X
eurjchem-1369	387	2	.	.	X
eurjchem-1369	387	3	conclusion	conclusion	NOUN
eurjchem-1369	387	4	in	in	ADP
eurjchem-1369	387	5	conclusion	conclusion	NOUN
eurjchem-1369	387	6	,	,	PUNCT
eurjchem-1369	387	7	a	a	DET
eurjchem-1369	387	8	series	series	NOUN
eurjchem-1369	387	9	of	of	ADP
eurjchem-1369	387	10	new	new	ADJ
eurjchem-1369	387	11	heterocyclic	heterocyclic	ADJ
eurjchem-1369	387	12	derivatives	derivative	NOUN
eurjchem-1369	387	13	of	of	ADP
eurjchem-1369	387	14	condensed	condense	VERB
eurjchem-1369	387	15	pyrazolopyrimidine	pyrazolopyrimidine	ADJ
eurjchem-1369	387	16	,	,	PUNCT
eurjchem-1369	387	17	pyrazoloquinazoline	pyrazoloquinazoline	ADJ
eurjchem-1369	387	18	and	and	CCONJ
eurjchem-1369	387	19	pyrazolotriazine	pyrazolotriazine	NOUN
eurjchem-1369	387	20	derivatives	derivative	NOUN
eurjchem-1369	387	21	starting	start	VERB
eurjchem-1369	387	22	with	with	ADP
eurjchem-1369	387	23	the	the	DET
eurjchem-1369	387	24	cyclic	cyclic	PROPN
eurjchem-1369	387	25	amidine	amidine	PROPN
eurjchem-1369	387	26	4a	4a	NOUN
eurjchem-1369	387	27	were	be	AUX
eurjchem-1369	387	28	synthesized	synthesize	VERB
eurjchem-1369	387	29	.	.	PUNCT
eurjchem-1369	388	1	the	the	DET
eurjchem-1369	388	2	structures	structure	NOUN
eurjchem-1369	388	3	of	of	ADP
eurjchem-1369	388	4	the	the	DET
eurjchem-1369	388	5	newly	newly	ADV
eurjchem-1369	388	6	synthesized	synthesize	VERB
eurjchem-1369	388	7	compounds	compound	NOUN
eurjchem-1369	388	8	were	be	AUX
eurjchem-1369	388	9	established	establish	VERB
eurjchem-1369	388	10	on	on	ADP
eurjchem-1369	388	11	the	the	DET
eurjchem-1369	388	12	basis	basis	NOUN
eurjchem-1369	388	13	of	of	ADP
eurjchem-1369	388	14	their	their	PRON
eurjchem-1369	388	15	spectral	spectral	ADJ
eurjchem-1369	388	16	data	datum	NOUN
eurjchem-1369	388	17	(	(	PUNCT
eurjchem-1369	388	18	ir	ir	PROPN
eurjchem-1369	388	19	,	,	PUNCT
eurjchem-1369	388	20	1h	1h	NUM
eurjchem-1369	388	21	nmr	nmr	NOUN
eurjchem-1369	388	22	,	,	PUNCT
eurjchem-1369	388	23	13c	13c	NOUN
eurjchem-1369	388	24	nmr	nmr	NOUN
eurjchem-1369	388	25	,	,	PUNCT
eurjchem-1369	388	26	mass	mass	PROPN
eurjchem-1369	388	27	)	)	PUNCT
eurjchem-1369	388	28	and	and	CCONJ
eurjchem-1369	388	29	elemental	elemental	ADJ
eurjchem-1369	388	30	analyses	analysis	NOUN
eurjchem-1369	388	31	.	.	PUNCT
eurjchem-1369	389	1	acknowledgement	acknowledgement	NOUN
eurjchem-1369	389	2	the	the	DET
eurjchem-1369	389	3	authors	author	NOUN
eurjchem-1369	389	4	are	be	AUX
eurjchem-1369	389	5	grateful	grateful	ADJ
eurjchem-1369	389	6	to	to	ADP
eurjchem-1369	389	7	south	south	PROPN
eurjchem-1369	389	8	valley	valley	PROPN
eurjchem-1369	389	9	university	university	PROPN
eurjchem-1369	389	10	,	,	PUNCT
eurjchem-1369	389	11	qena	qena	PROPN
eurjchem-1369	389	12	,	,	PUNCT
eurjchem-1369	389	13	egypt	egypt	PROPN
eurjchem-1369	389	14	for	for	ADP
eurjchem-1369	389	15	help	help	NOUN
eurjchem-1369	389	16	and	and	CCONJ
eurjchem-1369	389	17	support	support	NOUN
eurjchem-1369	389	18	.	.	PUNCT
eurjchem-1369	390	1	references	reference	NOUN
eurjchem-1369	390	2	[	[	X
eurjchem-1369	390	3	1	1	NUM
eurjchem-1369	390	4	]	]	PUNCT
eurjchem-1369	390	5	.	.	PUNCT
eurjchem-1369	391	1	marcos	marcos	PROPN
eurjchem-1369	391	2	,	,	PUNCT
eurjchem-1369	391	3	p.	p.	NOUN
eurjchem-1369	391	4	m.	m.	NOUN
eurjchem-1369	391	5	;	;	PUNCT
eurjchem-1369	391	6	elisandra	elisandra	PROPN
eurjchem-1369	391	7	,	,	PUNCT
eurjchem-1369	391	8	s.	s.	PROPN
eurjchem-1369	391	9	;	;	PUNCT
eurjchem-1369	391	10	clarissa	clarissa	PROPN
eurjchem-1369	391	11	,	,	PUNCT
eurjchem-1369	391	12	p.	p.	PROPN
eurjchem-1369	391	13	f.	f.	PROPN
eurjchem-1369	391	14	;	;	PUNCT
eurjchem-1369	391	15	fernanda	fernanda	PROPN
eurjchem-1369	391	16	,	,	PUNCT
eurjchem-1369	391	17	a.	a.	PROPN
eurjchem-1369	391	18	r.	r.	PROPN
eurjchem-1369	391	19	;	;	PUNCT
eurjchem-1369	391	20	helio	helio	NOUN
eurjchem-1369	391	21	,	,	PUNCT
eurjchem-1369	391	22	g.	g.	PROPN
eurjchem-1369	391	23	b.	b.	PROPN
eurjchem-1369	391	24	;	;	PUNCT
eurjchem-1369	391	25	nilo	nilo	PROPN
eurjchem-1369	391	26	,	,	PUNCT
eurjchem-1369	391	27	z.	z.	PROPN
eurjchem-1369	391	28	j.	j.	PROPN
eurjchem-1369	391	29	braz	braz	PROPN
eurjchem-1369	391	30	.	.	PUNCT
eurjchem-1369	392	1	chem	chem	PROPN
eurjchem-1369	392	2	.	.	PUNCT
eurjchem-1369	393	1	soc	soc	PROPN
eurjchem-1369	393	2	.	.	PUNCT
eurjchem-1369	394	1	2009	2009	NUM
eurjchem-1369	394	2	,	,	PUNCT
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eurjchem-1369	394	4	)	)	PUNCT
eurjchem-1369	394	5	,	,	PUNCT
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eurjchem-1369	395	3	]	]	PUNCT
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eurjchem-1369	398	2	,	,	PUNCT
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eurjchem-1369	400	2	,	,	PUNCT
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eurjchem-1369	401	2	,	,	PUNCT
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eurjchem-1369	402	4	.	.	PUNCT
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eurjchem-1369	403	2	,	,	PUNCT
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eurjchem-1369	403	4	;	;	PUNCT
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eurjchem-1369	404	2	,	,	PUNCT
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eurjchem-1369	405	3	]	]	PUNCT
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eurjchem-1369	405	9	;	;	PUNCT
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eurjchem-1369	405	11	,	,	PUNCT
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eurjchem-1369	405	13	;	;	PUNCT
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eurjchem-1369	406	2	.	.	PUNCT
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eurjchem-1369	407	2	,	,	PUNCT
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eurjchem-1369	407	4	)	)	PUNCT
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eurjchem-1369	408	3	]	]	PUNCT
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eurjchem-1369	409	2	,	,	PUNCT
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eurjchem-1369	409	4	;	;	PUNCT
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eurjchem-1369	409	6	,	,	PUNCT
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eurjchem-1369	409	8	;	;	PUNCT
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eurjchem-1369	409	10	,	,	PUNCT
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eurjchem-1369	409	13	;	;	PUNCT
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eurjchem-1369	410	5	.	.	PUNCT
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eurjchem-1369	411	2	,	,	PUNCT
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eurjchem-1369	412	3	]	]	PUNCT
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eurjchem-1369	413	2	,	,	PUNCT
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eurjchem-1369	413	5	;	;	PUNCT
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eurjchem-1369	413	17	,	,	PUNCT
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eurjchem-1369	413	21	,	,	PUNCT
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eurjchem-1369	413	23	;	;	PUNCT
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eurjchem-1369	413	25	,	,	PUNCT
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eurjchem-1369	413	29	.	.	PUNCT
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eurjchem-1369	414	5	.	.	PUNCT
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eurjchem-1369	415	2	,	,	PUNCT
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eurjchem-1369	415	4	,	,	PUNCT
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eurjchem-1369	416	2	8	8	NUM
eurjchem-1369	416	3	]	]	SYM
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eurjchem-1369	416	18	;	;	PUNCT
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eurjchem-1369	416	20	,	,	PUNCT
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eurjchem-1369	416	24	.	.	PUNCT
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eurjchem-1369	417	5	.	.	PUNCT
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eurjchem-1369	418	7	.	.	PUNCT
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eurjchem-1369	419	16	)	)	PUNCT
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eurjchem-1369	422	10	;	;	PUNCT
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eurjchem-1369	422	13	e.	e.	PROPN
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eurjchem-1369	429	2	,	,	PUNCT
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eurjchem-1369	434	2	,	,	PUNCT
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eurjchem-1369	436	20	;	;	PUNCT
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eurjchem-1369	436	25	.	.	PUNCT
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eurjchem-1369	437	4	.	.	PUNCT
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eurjchem-1369	438	2	.	.	PUNCT
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eurjchem-1369	439	2	,	,	PUNCT
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eurjchem-1369	439	4	,	,	PUNCT
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eurjchem-1369	439	6	.	.	PUNCT
eurjchem-1369	440	1	[	[	X
eurjchem-1369	440	2	13	13	NUM
eurjchem-1369	440	3	]	]	PUNCT
eurjchem-1369	440	4	.	.	PUNCT
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eurjchem-1369	441	2	,	,	PUNCT
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eurjchem-1369	441	4	;	;	PUNCT
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eurjchem-1369	441	6	,	,	PUNCT
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eurjchem-1369	441	8	;	;	PUNCT
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eurjchem-1369	441	23	;	;	PUNCT
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eurjchem-1369	441	25	,	,	PUNCT
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eurjchem-1369	441	36	.	.	PUNCT
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eurjchem-1369	442	2	,	,	PUNCT
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eurjchem-1369	442	4	,	,	PUNCT
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eurjchem-1369	442	6	.	.	PUNCT
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eurjchem-1369	443	3	]	]	PUNCT
eurjchem-1369	443	4	.	.	PUNCT
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eurjchem-1369	444	5	;	;	PUNCT
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eurjchem-1369	444	10	;	;	PUNCT
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eurjchem-1369	444	12	,	,	PUNCT
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eurjchem-1369	444	15	;	;	PUNCT
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eurjchem-1369	444	17	,	,	PUNCT
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eurjchem-1369	444	25	;	;	PUNCT
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eurjchem-1369	444	27	,	,	PUNCT
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eurjchem-1369	444	30	;	;	PUNCT
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eurjchem-1369	444	32	,	,	PUNCT
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eurjchem-1369	444	35	;	;	PUNCT
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eurjchem-1369	444	42	,	,	PUNCT
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eurjchem-1369	444	47	,	,	PUNCT
eurjchem-1369	444	48	k.	k.	PROPN
eurjchem-1369	444	49	e.	e.	PROPN
eurjchem-1369	444	50	;	;	PUNCT
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eurjchem-1369	444	54	a.	a.	PROPN
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eurjchem-1369	444	56	.	.	PUNCT
eurjchem-1369	445	1	med	med	PROPN
eurjchem-1369	445	2	.	.	PROPN
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eurjchem-1369	445	4	.	.	PUNCT
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eurjchem-1369	446	2	.	.	PUNCT
eurjchem-1369	446	3	2002	2002	NUM
eurjchem-1369	446	4	,	,	PUNCT
eurjchem-1369	446	5	12(19	12(19	NUM
eurjchem-1369	446	6	)	)	PUNCT
eurjchem-1369	446	7	,	,	PUNCT
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eurjchem-1369	446	9	.	.	PUNCT
eurjchem-1369	447	1	[	[	X
eurjchem-1369	447	2	15	15	NUM
eurjchem-1369	447	3	]	]	PUNCT
eurjchem-1369	447	4	.	.	PUNCT
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eurjchem-1369	448	2	,	,	PUNCT
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eurjchem-1369	448	5	;	;	PUNCT
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eurjchem-1369	448	7	,	,	PUNCT
eurjchem-1369	448	8	f.	f.	PROPN
eurjchem-1369	448	9	h.	h.	PROPN
eurjchem-1369	448	10	;	;	PUNCT
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eurjchem-1369	448	15	;	;	PUNCT
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eurjchem-1369	448	25	;	;	PUNCT
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eurjchem-1369	448	40	;	;	PUNCT
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eurjchem-1369	448	45	;	;	PUNCT
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eurjchem-1369	448	47	,	,	PUNCT
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eurjchem-1369	448	50	;	;	PUNCT
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eurjchem-1369	448	56	.	.	PUNCT
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eurjchem-1369	449	4	.	.	PUNCT
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eurjchem-1369	450	2	.	.	PUNCT
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eurjchem-1369	451	2	,	,	PUNCT
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eurjchem-1369	451	4	,	,	PUNCT
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eurjchem-1369	451	6	.	.	PUNCT
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eurjchem-1369	452	3	]	]	PUNCT
eurjchem-1369	452	4	.	.	PUNCT
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eurjchem-1369	453	2	,	,	PUNCT
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eurjchem-1369	453	4	;	;	PUNCT
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eurjchem-1369	453	13	.	.	PUNCT
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eurjchem-1369	454	2	,	,	PUNCT
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eurjchem-1369	454	4	,	,	PUNCT
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eurjchem-1369	454	6	.	.	PUNCT
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eurjchem-1369	455	3	]	]	PUNCT
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eurjchem-1369	455	12	;	;	PUNCT
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eurjchem-1369	456	2	,	,	PUNCT
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eurjchem-1369	457	4	.	.	PUNCT
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eurjchem-1369	458	2	,	,	PUNCT
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eurjchem-1369	458	4	;	;	PUNCT
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eurjchem-1369	458	10	.	.	PUNCT
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eurjchem-1369	459	4	,	,	PUNCT
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eurjchem-1369	460	15	.	.	PUNCT
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eurjchem-1369	464	2	,	,	PUNCT
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eurjchem-1369	466	18	.	.	PUNCT
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eurjchem-1369	467	2	.	.	PUNCT
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eurjchem-1369	468	2	,	,	PUNCT
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eurjchem-1369	470	5	;	;	PUNCT
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eurjchem-1369	481	6	)	)	PUNCT
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eurjchem-1369	485	6	.	.	PUNCT
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eurjchem-1369	486	3	,	,	PUNCT
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eurjchem-1369	486	5	,	,	PUNCT
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eurjchem-1369	486	7	.	.	PUNCT
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eurjchem-1369	487	2	26	26	NUM
eurjchem-1369	487	3	]	]	PUNCT
eurjchem-1369	487	4	.	.	PUNCT
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eurjchem-1369	488	2	,	,	PUNCT
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eurjchem-1369	488	5	;	;	PUNCT
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eurjchem-1369	490	2	,	,	PUNCT
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eurjchem-1369	490	4	)	)	PUNCT
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eurjchem-1369	490	7	.	.	PUNCT
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eurjchem-1369	492	2	,	,	PUNCT
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eurjchem-1369	492	4	;	;	PUNCT
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eurjchem-1369	494	2	,	,	PUNCT
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