id	sid	tid	token	lemma	pos
eurjchem-1434	1	1	untitled	untitle	VERB
eurjchem-1434	1	2	european	european	PROPN
eurjchem-1434	1	3	journal	journal	PROPN
eurjchem-1434	1	4	of	of	ADP
eurjchem-1434	1	5	chemistry	chemistry	NOUN
eurjchem-1434	1	6	7	7	NUM
eurjchem-1434	1	7	(	(	PUNCT
eurjchem-1434	1	8	2	2	NUM
eurjchem-1434	1	9	)	)	PUNCT
eurjchem-1434	1	10	(	(	PUNCT
eurjchem-1434	1	11	2016	2016	NUM
eurjchem-1434	1	12	)	)	PUNCT
eurjchem-1434	1	13	213‐216	213‐216	NUM
eurjchem-1434	1	14	european	european	PROPN
eurjchem-1434	1	15	journal	journal	PROPN
eurjchem-1434	1	16	of	of	ADP
eurjchem-1434	1	17	chemistry	chemistry	NOUN
eurjchem-1434	1	18	issn	issn	PROPN
eurjchem-1434	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-1434	1	20	(	(	PUNCT
eurjchem-1434	1	21	print	print	NOUN
eurjchem-1434	1	22	)	)	PUNCT
eurjchem-1434	1	23	/	/	SYM
eurjchem-1434	1	24	issn	issn	PROPN
eurjchem-1434	1	25	2153‐2257	2153‐2257	NUM
eurjchem-1434	1	26	(	(	PUNCT
eurjchem-1434	1	27	online	online	ADJ
eurjchem-1434	1	28	)	)	PUNCT
eurjchem-1434	1	29			NOUN
eurjchem-1434	1	30	2016	2016	NUM
eurjchem-1434	1	31	atlanta	atlanta	PROPN
eurjchem-1434	1	32	publishing	publishing	PROPN
eurjchem-1434	1	33	house	house	PROPN
eurjchem-1434	1	34	llc	llc	PROPN
eurjchem-1434	1	35	‐	‐	PUNCT
eurjchem-1434	1	36	all	all	DET
eurjchem-1434	1	37	rights	right	NOUN
eurjchem-1434	1	38	reserved	reserve	VERB
eurjchem-1434	1	39	‐	‐	NOUN
eurjchem-1434	1	40	printed	print	VERB
eurjchem-1434	1	41	in	in	ADP
eurjchem-1434	1	42	the	the	DET
eurjchem-1434	1	43	usa	usa	PROPN
eurjchem-1434	1	44	http://dx.doi.org/10.5155/eurjchem.7.2.213‐216.1434	http://dx.doi.org/10.5155/eurjchem.7.2.213‐216.1434	PROPN
eurjchem-1434	1	45	european	european	PROPN
eurjchem-1434	1	46	journal	journal	PROPN
eurjchem-1434	1	47	of	of	ADP
eurjchem-1434	1	48	chemistry	chemistry	PROPN
eurjchem-1434	1	49	journal	journal	PROPN
eurjchem-1434	1	50	webpage	webpage	NOUN
eurjchem-1434	1	51	:	:	PUNCT
eurjchem-1434	1	52	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1434	1	53	ultra‐performance	ultra‐performance	ADP
eurjchem-1434	1	54	liquid	liquid	ADJ
eurjchem-1434	1	55	chromatography	chromatography	NOUN
eurjchem-1434	1	56	coupled	couple	VERB
eurjchem-1434	1	57	to	to	PART
eurjchem-1434	1	58	electrospray	electrospray	VERB
eurjchem-1434	1	59	ionization‐	ionization‐	ADJ
eurjchem-1434	1	60	tandem	tandem	PROPN
eurjchem-1434	1	61	mass	mass	PROPN
eurjchem-1434	1	62	spectrometric	spectrometric	ADJ
eurjchem-1434	1	63	method	method	NOUN
eurjchem-1434	1	64	for	for	ADP
eurjchem-1434	1	65	simultaneous	simultaneous	ADJ
eurjchem-1434	1	66	determination	determination	NOUN
eurjchem-1434	1	67	of	of	ADP
eurjchem-1434	1	68	acemetacin	acemetacin	NOUN
eurjchem-1434	1	69	in	in	ADP
eurjchem-1434	1	70	presence	presence	NOUN
eurjchem-1434	1	71	of	of	ADP
eurjchem-1434	1	72	its	its	PRON
eurjchem-1434	1	73	metabolite	metabolite	NOUN
eurjchem-1434	1	74	indomethacin	indomethacin	NOUN
eurjchem-1434	1	75	and	and	CCONJ
eurjchem-1434	1	76	degradation	degradation	NOUN
eurjchem-1434	1	77	products	product	NOUN
eurjchem-1434	1	78	maha	maha	PROPN
eurjchem-1434	1	79	mahmoud	mahmoud	PROPN
eurjchem-1434	2	1	abou‐el	abou‐el	PROPN
eurjchem-1434	2	2	alamin	alamin	PROPN
eurjchem-1434	2	3	analytical	analytical	ADJ
eurjchem-1434	2	4	chemistry	chemistry	NOUN
eurjchem-1434	2	5	department	department	NOUN
eurjchem-1434	2	6	,	,	PUNCT
eurjchem-1434	2	7	faculty	faculty	NOUN
eurjchem-1434	2	8	of	of	ADP
eurjchem-1434	2	9	pharmacy	pharmacy	NOUN
eurjchem-1434	2	10	,	,	PUNCT
eurjchem-1434	2	11	helwan	helwan	PROPN
eurjchem-1434	2	12	university	university	PROPN
eurjchem-1434	2	13	,	,	PUNCT
eurjchem-1434	2	14	11795	11795	NUM
eurjchem-1434	2	15	,	,	PUNCT
eurjchem-1434	2	16	cairo	cairo	PROPN
eurjchem-1434	2	17	,	,	PUNCT
eurjchem-1434	2	18	egypt	egypt	PROPN
eurjchem-1434	2	19	*	*	PUNCT
eurjchem-1434	2	20	corresponding	correspond	VERB
eurjchem-1434	2	21	author	author	NOUN
eurjchem-1434	2	22	at	at	ADP
eurjchem-1434	2	23	:	:	PUNCT
eurjchem-1434	2	24	analytical	analytical	ADJ
eurjchem-1434	2	25	chemistry	chemistry	NOUN
eurjchem-1434	2	26	department	department	NOUN
eurjchem-1434	2	27	,	,	PUNCT
eurjchem-1434	2	28	faculty	faculty	NOUN
eurjchem-1434	2	29	of	of	ADP
eurjchem-1434	2	30	pharmacy	pharmacy	NOUN
eurjchem-1434	2	31	,	,	PUNCT
eurjchem-1434	2	32	helwan	helwan	PROPN
eurjchem-1434	2	33	university	university	PROPN
eurjchem-1434	2	34	,	,	PUNCT
eurjchem-1434	2	35	11795	11795	NUM
eurjchem-1434	2	36	,	,	PUNCT
eurjchem-1434	2	37	cairo	cairo	PROPN
eurjchem-1434	2	38	,	,	PUNCT
eurjchem-1434	2	39	egypt	egypt	PROPN
eurjchem-1434	2	40	.	.	PUNCT
eurjchem-1434	3	1	tel	tel	PROPN
eurjchem-1434	3	2	.	.	PROPN
eurjchem-1434	3	3	:	:	PUNCT
eurjchem-1434	4	1	+2.02.25541601	+2.02.25541601	PROPN
eurjchem-1434	4	2	.	.	PUNCT
eurjchem-1434	4	3	fax	fax	NOUN
eurjchem-1434	4	4	:	:	PUNCT
eurjchem-1434	4	5	+2.02.25541601	+2.02.25541601	PROPN
eurjchem-1434	4	6	.	.	PUNCT
eurjchem-1434	4	7	e‐mail	e‐mail	PUNCT
eurjchem-1434	4	8	address	address	NOUN
eurjchem-1434	4	9	:	:	PUNCT
eurjchem-1434	4	10	dr.maha.alamin@gmail.com	dr.maha.alamin@gmail.com	PROPN
eurjchem-1434	4	11	(	(	PUNCT
eurjchem-1434	4	12	m.m.a	m.m.a	NOUN
eurjchem-1434	4	13	.	.	PUNCT
eurjchem-1434	4	14	el‐alamin	el‐alamin	PROPN
eurjchem-1434	4	15	)	)	PUNCT
eurjchem-1434	4	16	.	.	PUNCT
eurjchem-1434	5	1	article	article	NOUN
eurjchem-1434	5	2	information	information	PROPN
eurjchem-1434	5	3	abstract	abstract	ADJ
eurjchem-1434	5	4	doi	doi	NOUN
eurjchem-1434	5	5	:	:	PUNCT
eurjchem-1434	5	6	10.5155	10.5155	NUM
eurjchem-1434	5	7	/	/	SYM
eurjchem-1434	5	8	eurjchem.7.2.213‐216.1434	eurjchem.7.2.213‐216.1434	PRON
eurjchem-1434	5	9	received	receive	VERB
eurjchem-1434	5	10	:	:	PUNCT
eurjchem-1434	5	11	02	02	NUM
eurjchem-1434	5	12	april	april	PROPN
eurjchem-1434	5	13	2016	2016	NUM
eurjchem-1434	5	14	received	receive	VERB
eurjchem-1434	5	15	in	in	ADP
eurjchem-1434	5	16	revised	revise	VERB
eurjchem-1434	5	17	form	form	NOUN
eurjchem-1434	5	18	:	:	PUNCT
eurjchem-1434	5	19	23	23	NUM
eurjchem-1434	5	20	april	april	PROPN
eurjchem-1434	5	21	2016	2016	NUM
eurjchem-1434	5	22	accepted	accept	VERB
eurjchem-1434	5	23	:	:	PUNCT
eurjchem-1434	5	24	29	29	NUM
eurjchem-1434	5	25	april	april	PROPN
eurjchem-1434	5	26	2016	2016	NUM
eurjchem-1434	5	27	published	publish	VERB
eurjchem-1434	5	28	online	online	ADV
eurjchem-1434	5	29	:	:	PUNCT
eurjchem-1434	5	30	30	30	NUM
eurjchem-1434	5	31	june	june	PROPN
eurjchem-1434	5	32	2016	2016	NUM
eurjchem-1434	5	33	printed	print	VERB
eurjchem-1434	5	34	:	:	PUNCT
eurjchem-1434	5	35	30	30	NUM
eurjchem-1434	5	36	june	june	PROPN
eurjchem-1434	5	37	2016	2016	NUM
eurjchem-1434	5	38	selective	selective	ADJ
eurjchem-1434	5	39	and	and	CCONJ
eurjchem-1434	5	40	sensitive	sensitive	ADJ
eurjchem-1434	5	41	ultra‐performance	ultra‐performance	ADP
eurjchem-1434	5	42	liquid	liquid	ADJ
eurjchem-1434	5	43	chromatography‐tandem	chromatography‐tandem	PROPN
eurjchem-1434	5	44	mass	mass	NOUN
eurjchem-1434	5	45	spectrometric	spectrometric	ADJ
eurjchem-1434	5	46	technique	technique	NOUN
eurjchem-1434	5	47	(	(	PUNCT
eurjchem-1434	5	48	uplc‐ms	uplc‐ms	NOUN
eurjchem-1434	5	49	/	/	SYM
eurjchem-1434	5	50	ms	ms	NOUN
eurjchem-1434	5	51	)	)	PUNCT
eurjchem-1434	5	52	was	be	AUX
eurjchem-1434	5	53	investigated	investigate	VERB
eurjchem-1434	5	54	for	for	ADP
eurjchem-1434	5	55	simultaneous	simultaneous	ADJ
eurjchem-1434	5	56	determination	determination	NOUN
eurjchem-1434	5	57	of	of	ADP
eurjchem-1434	5	58	acemetacin	acemetacin	PROPN
eurjchem-1434	5	59	(	(	PUNCT
eurjchem-1434	5	60	acm	acm	PROPN
eurjchem-1434	5	61	)	)	PUNCT
eurjchem-1434	5	62	in	in	ADP
eurjchem-1434	5	63	presence	presence	NOUN
eurjchem-1434	5	64	of	of	ADP
eurjchem-1434	5	65	its	its	PRON
eurjchem-1434	5	66	metabolite	metabolite	NOUN
eurjchem-1434	5	67	(	(	PUNCT
eurjchem-1434	5	68	indomethacin	indomethacin	PROPN
eurjchem-1434	5	69	)	)	PUNCT
eurjchem-1434	5	70	and	and	CCONJ
eurjchem-1434	5	71	degradation	degradation	NOUN
eurjchem-1434	5	72	products	product	NOUN
eurjchem-1434	5	73	in	in	ADP
eurjchem-1434	5	74	3	3	NUM
eurjchem-1434	5	75	min	min	NOUN
eurjchem-1434	5	76	run	run	NOUN
eurjchem-1434	5	77	time	time	NOUN
eurjchem-1434	5	78	.	.	PUNCT
eurjchem-1434	6	1	the	the	DET
eurjchem-1434	6	2	column	column	NOUN
eurjchem-1434	6	3	employed	employ	VERB
eurjchem-1434	6	4	was	be	AUX
eurjchem-1434	6	5	a	a	DET
eurjchem-1434	6	6	hypersil	hypersil	NOUN
eurjchem-1434	6	7	gold	gold	NOUN
eurjchem-1434	6	8	50	50	NUM
eurjchem-1434	6	9	mm	mm	NOUN
eurjchem-1434	6	10	×	×	NOUN
eurjchem-1434	6	11	2.1	2.1	NUM
eurjchem-1434	6	12	mm	mm	NOUN
eurjchem-1434	6	13	(	(	PUNCT
eurjchem-1434	6	14	1.9	1.9	NUM
eurjchem-1434	6	15	μm	μm	NUM
eurjchem-1434	6	16	)	)	PUNCT
eurjchem-1434	6	17	with	with	ADP
eurjchem-1434	6	18	an	an	DET
eurjchem-1434	6	19	isocratic	isocratic	ADJ
eurjchem-1434	6	20	mobile	mobile	ADJ
eurjchem-1434	6	21	phase	phase	NOUN
eurjchem-1434	6	22	consisted	consist	VERB
eurjchem-1434	6	23	of	of	ADP
eurjchem-1434	6	24	0.1	0.1	NUM
eurjchem-1434	6	25	%	%	NOUN
eurjchem-1434	6	26	formic	formic	ADJ
eurjchem-1434	6	27	acid	acid	NOUN
eurjchem-1434	6	28	aqueous	aqueous	ADJ
eurjchem-1434	6	29	solution	solution	NOUN
eurjchem-1434	6	30	and	and	CCONJ
eurjchem-1434	6	31	acetonitrile	acetonitrile	NOUN
eurjchem-1434	6	32	(	(	PUNCT
eurjchem-1434	6	33	10:90	10:90	NUM
eurjchem-1434	6	34	,	,	PUNCT
eurjchem-1434	6	35	v	v	NOUN
eurjchem-1434	6	36	:	:	PUNCT
eurjchem-1434	6	37	v	v	NOUN
eurjchem-1434	6	38	)	)	PUNCT
eurjchem-1434	6	39	with	with	ADP
eurjchem-1434	6	40	flow	flow	NOUN
eurjchem-1434	6	41	rate	rate	NOUN
eurjchem-1434	6	42	250	250	NUM
eurjchem-1434	6	43	µl	µl	NOUN
eurjchem-1434	6	44	/	/	SYM
eurjchem-1434	6	45	min	min	NOUN
eurjchem-1434	6	46	.	.	PROPN
eurjchem-1434	6	47	detection	detection	NOUN
eurjchem-1434	6	48	of	of	ADP
eurjchem-1434	6	49	the	the	DET
eurjchem-1434	6	50	cited	cite	VERB
eurjchem-1434	6	51	drug	drug	NOUN
eurjchem-1434	6	52	was	be	AUX
eurjchem-1434	6	53	carried	carry	VERB
eurjchem-1434	6	54	out	out	ADP
eurjchem-1434	6	55	using	use	VERB
eurjchem-1434	6	56	multiple	multiple	ADJ
eurjchem-1434	6	57	reaction	reaction	NOUN
eurjchem-1434	6	58	monitoring	monitoring	NOUN
eurjchem-1434	6	59	(	(	PUNCT
eurjchem-1434	6	60	mrm	mrm	PROPN
eurjchem-1434	6	61	)	)	PUNCT
eurjchem-1434	6	62	mode	mode	NOUN
eurjchem-1434	6	63	on	on	ADP
eurjchem-1434	6	64	a	a	DET
eurjchem-1434	6	65	triple	triple	ADJ
eurjchem-1434	6	66	quadrupole	quadrupole	NOUN
eurjchem-1434	6	67	mass	mass	NOUN
eurjchem-1434	6	68	spectrometer	spectrometer	NOUN
eurjchem-1434	6	69	coupled	couple	VERB
eurjchem-1434	6	70	with	with	ADP
eurjchem-1434	6	71	electrospray	electrospray	NOUN
eurjchem-1434	6	72	ionization	ionization	NOUN
eurjchem-1434	6	73	(	(	PUNCT
eurjchem-1434	6	74	esi	esi	NOUN
eurjchem-1434	6	75	)	)	PUNCT
eurjchem-1434	6	76	m	m	PROPN
eurjchem-1434	6	77	/	/	SYM
eurjchem-1434	6	78	z	z	PROPN
eurjchem-1434	6	79	416.44	416.44	NUM
eurjchem-1434	6	80	→	→	SYM
eurjchem-1434	6	81	139.24	139.24	NUM
eurjchem-1434	6	82	for	for	ADP
eurjchem-1434	6	83	acm	acm	NOUN
eurjchem-1434	6	84	and	and	CCONJ
eurjchem-1434	6	85	m	m	PROPN
eurjchem-1434	6	86	/	/	SYM
eurjchem-1434	6	87	z	z	PROPN
eurjchem-1434	6	88	256.31	256.31	NUM
eurjchem-1434	6	89	→	→	SYM
eurjchem-1434	6	90	167.00	167.00	NUM
eurjchem-1434	6	91	for	for	ADP
eurjchem-1434	6	92	diphenhydramine	diphenhydramine	ADJ
eurjchem-1434	6	93	internal	internal	ADJ
eurjchem-1434	6	94	standard	standard	PROPN
eurjchem-1434	6	95	.	.	PUNCT
eurjchem-1434	7	1	various	various	ADJ
eurjchem-1434	7	2	parameters	parameter	NOUN
eurjchem-1434	7	3	were	be	AUX
eurjchem-1434	7	4	studied	study	VERB
eurjchem-1434	7	5	;	;	PUNCT
eurjchem-1434	7	6	mobile	mobile	ADJ
eurjchem-1434	7	7	phase	phase	NOUN
eurjchem-1434	7	8	composition	composition	NOUN
eurjchem-1434	7	9	,	,	PUNCT
eurjchem-1434	7	10	flow	flow	NOUN
eurjchem-1434	7	11	rate	rate	NOUN
eurjchem-1434	7	12	,	,	PUNCT
eurjchem-1434	7	13	rate	rate	NOUN
eurjchem-1434	7	14	of	of	ADP
eurjchem-1434	7	15	fragmentation	fragmentation	NOUN
eurjchem-1434	7	16	,	,	PUNCT
eurjchem-1434	7	17	rate	rate	NOUN
eurjchem-1434	7	18	of	of	ADP
eurjchem-1434	7	19	collision	collision	NOUN
eurjchem-1434	7	20	and	and	CCONJ
eurjchem-1434	7	21	mode	mode	NOUN
eurjchem-1434	7	22	of	of	ADP
eurjchem-1434	7	23	ionization	ionization	NOUN
eurjchem-1434	7	24	.	.	PUNCT
eurjchem-1434	8	1	good	good	ADJ
eurjchem-1434	8	2	linear	linear	PROPN
eurjchem-1434	8	3	relationship	relationship	NOUN
eurjchem-1434	8	4	was	be	AUX
eurjchem-1434	8	5	obtained	obtain	VERB
eurjchem-1434	8	6	in	in	ADP
eurjchem-1434	8	7	concentration	concentration	NOUN
eurjchem-1434	8	8	range	range	NOUN
eurjchem-1434	8	9	8.0‐500.0	8.0‐500.0	PROPN
eurjchem-1434	8	10	ng	ng	PROPN
eurjchem-1434	8	11	/	/	SYM
eurjchem-1434	8	12	ml	ml	PROPN
eurjchem-1434	8	13	(	(	PUNCT
eurjchem-1434	8	14	r	r	NOUN
eurjchem-1434	8	15	=	=	SYM
eurjchem-1434	8	16	0.9994	0.9994	NUM
eurjchem-1434	8	17	)	)	PUNCT
eurjchem-1434	8	18	.	.	PUNCT
eurjchem-1434	9	1	the	the	DET
eurjchem-1434	9	2	method	method	NOUN
eurjchem-1434	9	3	was	be	AUX
eurjchem-1434	9	4	validated	validate	VERB
eurjchem-1434	9	5	(	(	PUNCT
eurjchem-1434	9	6	linearity	linearity	NOUN
eurjchem-1434	9	7	,	,	PUNCT
eurjchem-1434	9	8	range	range	NOUN
eurjchem-1434	9	9	,	,	PUNCT
eurjchem-1434	9	10	precision	precision	NOUN
eurjchem-1434	9	11	,	,	PUNCT
eurjchem-1434	9	12	accuracy	accuracy	NOUN
eurjchem-1434	9	13	,	,	PUNCT
eurjchem-1434	9	14	limit	limit	NOUN
eurjchem-1434	9	15	of	of	ADP
eurjchem-1434	9	16	quantification	quantification	NOUN
eurjchem-1434	9	17	and	and	CCONJ
eurjchem-1434	9	18	limit	limit	NOUN
eurjchem-1434	9	19	of	of	ADP
eurjchem-1434	9	20	detection	detection	NOUN
eurjchem-1434	9	21	)	)	PUNCT
eurjchem-1434	9	22	according	accord	VERB
eurjchem-1434	9	23	to	to	ADP
eurjchem-1434	9	24	ich	ich	NOUN
eurjchem-1434	9	25	guidelines	guideline	NOUN
eurjchem-1434	9	26	and	and	CCONJ
eurjchem-1434	9	27	there	there	PRON
eurjchem-1434	9	28	is	be	VERB
eurjchem-1434	9	29	no	no	DET
eurjchem-1434	9	30	significance	significance	NOUN
eurjchem-1434	9	31	difference	difference	NOUN
eurjchem-1434	9	32	between	between	ADP
eurjchem-1434	9	33	the	the	DET
eurjchem-1434	9	34	proposed	propose	VERB
eurjchem-1434	9	35	method	method	NOUN
eurjchem-1434	9	36	and	and	CCONJ
eurjchem-1434	9	37	the	the	DET
eurjchem-1434	9	38	reference	reference	NOUN
eurjchem-1434	9	39	hplc	hplc	NOUN
eurjchem-1434	9	40	method	method	NOUN
eurjchem-1434	9	41	regarding	regard	VERB
eurjchem-1434	9	42	accuracy	accuracy	NOUN
eurjchem-1434	9	43	and	and	CCONJ
eurjchem-1434	9	44	precision	precision	NOUN
eurjchem-1434	9	45	.	.	PUNCT
eurjchem-1434	10	1	the	the	DET
eurjchem-1434	10	2	simplicity	simplicity	NOUN
eurjchem-1434	10	3	and	and	CCONJ
eurjchem-1434	10	4	sensitivity	sensitivity	NOUN
eurjchem-1434	10	5	of	of	ADP
eurjchem-1434	10	6	this	this	DET
eurjchem-1434	10	7	method	method	NOUN
eurjchem-1434	10	8	allows	allow	VERB
eurjchem-1434	10	9	its	its	PRON
eurjchem-1434	10	10	use	use	NOUN
eurjchem-1434	10	11	as	as	ADP
eurjchem-1434	10	12	stability	stability	NOUN
eurjchem-1434	10	13	indicating	indicate	VERB
eurjchem-1434	10	14	method	method	NOUN
eurjchem-1434	10	15	.	.	PUNCT
eurjchem-1434	11	1	keywords	keyword	NOUN
eurjchem-1434	11	2	uplc	uplc	VERB
eurjchem-1434	11	3	validation	validation	NOUN
eurjchem-1434	11	4	acemetacin	acemetacin	ADV
eurjchem-1434	11	5	indomethacin	indomethacin	VERB
eurjchem-1434	11	6	tandem	tandem	PROPN
eurjchem-1434	11	7	mass	mass	PROPN
eurjchem-1434	11	8	stability	stability	NOUN
eurjchem-1434	11	9	indicating	indicate	VERB
eurjchem-1434	11	10	cite	cite	VERB
eurjchem-1434	11	11	this	this	PRON
eurjchem-1434	11	12	:	:	PUNCT
eurjchem-1434	11	13	eur	eur	PROPN
eurjchem-1434	11	14	.	.	PUNCT
eurjchem-1434	12	1	j.	j.	PROPN
eurjchem-1434	12	2	chem	chem	PROPN
eurjchem-1434	12	3	.	.	PUNCT
eurjchem-1434	13	1	2016	2016	NUM
eurjchem-1434	13	2	,	,	PUNCT
eurjchem-1434	13	3	7(2	7(2	NUM
eurjchem-1434	13	4	)	)	PUNCT
eurjchem-1434	13	5	,	,	PUNCT
eurjchem-1434	13	6	213‐216	213‐216	NUM
eurjchem-1434	13	7	1	1	NUM
eurjchem-1434	13	8	.	.	PUNCT
eurjchem-1434	13	9	introduction	introduction	NOUN
eurjchem-1434	13	10	acemetacin	acemetacin	PROPN
eurjchem-1434	13	11	acm	acm	PROPN
eurjchem-1434	13	12	,	,	PUNCT
eurjchem-1434	13	13	(	(	PUNCT
eurjchem-1434	13	14	2‐[2‐[1‐(4‐chlorobenzoyl)‐5‐methoxy‐	2‐[2‐[1‐(4‐chlorobenzoyl)‐5‐methoxy‐	NOUN
eurjchem-1434	13	15	2‐methylindol‐3‐yl	2‐methylindol‐3‐yl	NUM
eurjchem-1434	13	16	]	]	X
eurjchem-1434	13	17	acetyl]oxyacetic	acetyl]oxyacetic	PROPN
eurjchem-1434	13	18	acid	acid	NOUN
eurjchem-1434	13	19	)	)	PUNCT
eurjchem-1434	13	20	is	be	AUX
eurjchem-1434	13	21	a	a	DET
eurjchem-1434	13	22	non‐steroidal	non‐steroidal	ADJ
eurjchem-1434	13	23	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-1434	13	24	drug	drug	NOUN
eurjchem-1434	13	25	,	,	PUNCT
eurjchem-1434	13	26	used	use	VERB
eurjchem-1434	13	27	for	for	ADP
eurjchem-1434	13	28	the	the	DET
eurjchem-1434	13	29	treatment	treatment	NOUN
eurjchem-1434	13	30	of	of	ADP
eurjchem-1434	13	31	osteo‐	osteo‐	PROPN
eurjchem-1434	13	32	arthritis	arthritis	NOUN
eurjchem-1434	13	33	and	and	CCONJ
eurjchem-1434	13	34	rheumatoid	rheumatoid	VERB
eurjchem-1434	13	35	arthritis	arthritis	NOUN
eurjchem-1434	13	36	(	(	PUNCT
eurjchem-1434	13	37	figure	figure	NOUN
eurjchem-1434	13	38	1	1	NUM
eurjchem-1434	13	39	)	)	PUNCT
eurjchem-1434	13	40	.	.	PUNCT
eurjchem-1434	14	1	it	it	PRON
eurjchem-1434	14	2	is	be	AUX
eurjchem-1434	14	3	a	a	DET
eurjchem-1434	14	4	glycolic	glycolic	NOUN
eurjchem-1434	14	5	acid	acid	NOUN
eurjchem-1434	14	6	ester	ester	NOUN
eurjchem-1434	14	7	of	of	ADP
eurjchem-1434	14	8	indometacin	indometacin	NOUN
eurjchem-1434	14	9	,	,	PUNCT
eurjchem-1434	14	10	acts	act	VERB
eurjchem-1434	14	11	as	as	ADP
eurjchem-1434	14	12	a	a	DET
eurjchem-1434	14	13	prodrug	prodrug	NOUN
eurjchem-1434	14	14	;	;	PUNCT
eurjchem-1434	14	15	in	in	ADP
eurjchem-1434	14	16	the	the	DET
eurjchem-1434	14	17	body	body	NOUN
eurjchem-1434	14	18	,	,	PUNCT
eurjchem-1434	14	19	it	it	PRON
eurjchem-1434	14	20	is	be	AUX
eurjchem-1434	14	21	metabolized	metabolize	VERB
eurjchem-1434	14	22	to	to	ADP
eurjchem-1434	14	23	indomethacin	indomethacin	NOUN
eurjchem-1434	14	24	,	,	PUNCT
eurjchem-1434	14	25	which	which	PRON
eurjchem-1434	14	26	then	then	ADV
eurjchem-1434	14	27	acts	act	VERB
eurjchem-1434	14	28	as	as	ADP
eurjchem-1434	14	29	an	an	DET
eurjchem-1434	14	30	inhibitor	inhibitor	NOUN
eurjchem-1434	14	31	of	of	ADP
eurjchem-1434	14	32	cyclooxygenase	cyclooxygenase	NOUN
eurjchem-1434	14	33	,	,	PUNCT
eurjchem-1434	14	34	producing	produce	VERB
eurjchem-1434	14	35	the	the	DET
eurjchem-1434	14	36	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-1434	14	37	effects	effect	NOUN
eurjchem-1434	14	38	.	.	PUNCT
eurjchem-1434	15	1	an	an	DET
eurjchem-1434	15	2	advantage	advantage	NOUN
eurjchem-1434	15	3	of	of	ADP
eurjchem-1434	15	4	acemetacin	acemetacin	ADV
eurjchem-1434	15	5	is	be	AUX
eurjchem-1434	15	6	that	that	SCONJ
eurjchem-1434	15	7	it	it	PRON
eurjchem-1434	15	8	reduces	reduce	VERB
eurjchem-1434	15	9	gastric	gastric	ADJ
eurjchem-1434	15	10	damage	damage	NOUN
eurjchem-1434	15	11	when	when	SCONJ
eurjchem-1434	15	12	compared	compare	VERB
eurjchem-1434	15	13	to	to	ADP
eurjchem-1434	15	14	indomethacin	indomethacin	NOUN
eurjchem-1434	15	15	[	[	PUNCT
eurjchem-1434	15	16	1	1	NUM
eurjchem-1434	15	17	]	]	PUNCT
eurjchem-1434	15	18	.	.	PUNCT
eurjchem-1434	16	1	literature	literature	NOUN
eurjchem-1434	16	2	survey	survey	NOUN
eurjchem-1434	16	3	reveals	reveal	VERB
eurjchem-1434	16	4	that	that	SCONJ
eurjchem-1434	16	5	there	there	PRON
eurjchem-1434	16	6	are	be	VERB
eurjchem-1434	16	7	several	several	ADJ
eurjchem-1434	16	8	methods	method	NOUN
eurjchem-1434	16	9	have	have	AUX
eurjchem-1434	16	10	been	be	AUX
eurjchem-1434	16	11	investigated	investigate	VERB
eurjchem-1434	16	12	for	for	ADP
eurjchem-1434	16	13	the	the	DET
eurjchem-1434	16	14	determination	determination	NOUN
eurjchem-1434	16	15	of	of	ADP
eurjchem-1434	16	16	acm	acm	PROPN
eurjchem-1434	16	17	,	,	PUNCT
eurjchem-1434	16	18	such	such	ADJ
eurjchem-1434	16	19	as	as	ADP
eurjchem-1434	16	20	spectrophotometric	spectrophotometric	ADJ
eurjchem-1434	16	21	[	[	X
eurjchem-1434	16	22	2‐4	2‐4	NUM
eurjchem-1434	16	23	]	]	PUNCT
eurjchem-1434	16	24	,	,	PUNCT
eurjchem-1434	16	25	chromatographic	chromatographic	ADJ
eurjchem-1434	16	26	[	[	X
eurjchem-1434	16	27	2‐6	2‐6	X
eurjchem-1434	16	28	]	]	PUNCT
eurjchem-1434	16	29	and	and	CCONJ
eurjchem-1434	16	30	voltam‐	voltam‐	X
eurjchem-1434	16	31	metric	metric	ADJ
eurjchem-1434	16	32	methods	method	NOUN
eurjchem-1434	16	33	[	[	X
eurjchem-1434	16	34	7,8	7,8	NUM
eurjchem-1434	16	35	]	]	PUNCT
eurjchem-1434	16	36	.	.	PUNCT
eurjchem-1434	17	1	the	the	DET
eurjchem-1434	17	2	british	british	ADJ
eurjchem-1434	17	3	pharmacopoeia	pharmacopoeia	NOUN
eurjchem-1434	17	4	[	[	X
eurjchem-1434	17	5	9	9	NUM
eurjchem-1434	17	6	]	]	PUNCT
eurjchem-1434	17	7	described	describe	VERB
eurjchem-1434	17	8	indomethacin	indomethacin	NOUN
eurjchem-1434	17	9	and	and	CCONJ
eurjchem-1434	17	10	p‐chlorobenzoic	p‐chlorobenzoic	PUNCT
eurjchem-1434	17	11	acid	acid	NOUN
eurjchem-1434	17	12	(	(	PUNCT
eurjchem-1434	17	13	pcba	pcba	NOUN
eurjchem-1434	17	14	)	)	PUNCT
eurjchem-1434	17	15	as	as	ADP
eurjchem-1434	17	16	impurities	impurity	NOUN
eurjchem-1434	17	17	for	for	ADP
eurjchem-1434	17	18	acm	acm	NOUN
eurjchem-1434	17	19	.	.	PUNCT
eurjchem-1434	17	20	p‐chlorobenzoic	p‐chlorobenzoic	PUNCT
eurjchem-1434	17	21	acid	acid	ADJ
eurjchem-1434	17	22	and	and	CCONJ
eurjchem-1434	17	23	5‐methoxy‐	5‐methoxy‐	NOUN
eurjchem-1434	17	24	2‐methyl‐3‐indole	2‐methyl‐3‐indole	NUM
eurjchem-1434	17	25	acetic	acetic	ADJ
eurjchem-1434	17	26	acid	acid	NOUN
eurjchem-1434	17	27	are	be	AUX
eurjchem-1434	17	28	reported	report	VERB
eurjchem-1434	17	29	as	as	ADP
eurjchem-1434	17	30	the	the	DET
eurjchem-1434	17	31	degradation	degradation	NOUN
eurjchem-1434	17	32	products	product	NOUN
eurjchem-1434	17	33	under	under	ADP
eurjchem-1434	17	34	specific	specific	ADJ
eurjchem-1434	17	35	alkaline	alkaline	NOUN
eurjchem-1434	17	36	and	and	CCONJ
eurjchem-1434	17	37	acidic	acidic	ADJ
eurjchem-1434	17	38	stress	stress	NOUN
eurjchem-1434	17	39	conditions	condition	NOUN
eurjchem-1434	17	40	[	[	X
eurjchem-1434	17	41	5	5	NUM
eurjchem-1434	17	42	]	]	PUNCT
eurjchem-1434	17	43	.	.	PUNCT
eurjchem-1434	18	1	these	these	DET
eurjchem-1434	18	2	degradation	degradation	NOUN
eurjchem-1434	18	3	products	product	NOUN
eurjchem-1434	18	4	obtained	obtain	VERB
eurjchem-1434	18	5	were	be	AUX
eurjchem-1434	18	6	confirmed	confirm	VERB
eurjchem-1434	18	7	by	by	ADP
eurjchem-1434	18	8	their	their	PRON
eurjchem-1434	18	9	m	m	NOUN
eurjchem-1434	18	10	/	/	SYM
eurjchem-1434	18	11	z	z	NOUN
eurjchem-1434	18	12	using	use	VERB
eurjchem-1434	18	13	uplc‐ms	uplc‐ms	ADP
eurjchem-1434	18	14	/	/	SYM
eurjchem-1434	18	15	ms	ms	PROPN
eurjchem-1434	18	16	.	.	PROPN
eurjchem-1434	18	17	figure	figure	PROPN
eurjchem-1434	18	18	1	1	NUM
eurjchem-1434	18	19	.	.	PUNCT
eurjchem-1434	18	20	structure	structure	NOUN
eurjchem-1434	18	21	of	of	ADP
eurjchem-1434	18	22	acemetacin	acemetacin	ADV
eurjchem-1434	18	23	.	.	PUNCT
eurjchem-1434	19	1	to	to	ADP
eurjchem-1434	19	2	our	our	PRON
eurjchem-1434	19	3	knowledge	knowledge	NOUN
eurjchem-1434	19	4	,	,	PUNCT
eurjchem-1434	19	5	there	there	PRON
eurjchem-1434	19	6	is	be	VERB
eurjchem-1434	19	7	no	no	DET
eurjchem-1434	19	8	validated	validated	ADJ
eurjchem-1434	19	9	uplc‐ms	uplc‐ms	NOUN
eurjchem-1434	19	10	/	/	SYM
eurjchem-1434	19	11	ms	ms	NOUN
eurjchem-1434	19	12	method	method	NOUN
eurjchem-1434	19	13	was	be	AUX
eurjchem-1434	19	14	developed	develop	VERB
eurjchem-1434	19	15	for	for	ADP
eurjchem-1434	19	16	the	the	DET
eurjchem-1434	19	17	determination	determination	NOUN
eurjchem-1434	19	18	of	of	ADP
eurjchem-1434	19	19	acm	acm	NOUN
eurjchem-1434	19	20	in	in	ADP
eurjchem-1434	19	21	presence	presence	NOUN
eurjchem-1434	19	22	of	of	ADP
eurjchem-1434	19	23	its	its	PRON
eurjchem-1434	19	24	metabolite	metabolite	NOUN
eurjchem-1434	19	25	(	(	PUNCT
eurjchem-1434	19	26	indomethacin	indomethacin	PROPN
eurjchem-1434	19	27	)	)	PUNCT
eurjchem-1434	19	28	and	and	CCONJ
eurjchem-1434	19	29	degradation	degradation	NOUN
eurjchem-1434	19	30	products	product	NOUN
eurjchem-1434	19	31	.	.	PUNCT
eurjchem-1434	20	1	therefore	therefore	ADV
eurjchem-1434	20	2	,	,	PUNCT
eurjchem-1434	20	3	the	the	DET
eurjchem-1434	20	4	aim	aim	NOUN
eurjchem-1434	20	5	of	of	ADP
eurjchem-1434	20	6	this	this	DET
eurjchem-1434	20	7	paper	paper	NOUN
eurjchem-1434	20	8	was	be	AUX
eurjchem-1434	20	9	to	to	PART
eurjchem-1434	20	10	develop	develop	VERB
eurjchem-1434	20	11	a	a	DET
eurjchem-1434	20	12	validated	validate	VERB
eurjchem-1434	20	13	,	,	PUNCT
eurjchem-1434	20	14	sensitive	sensitive	ADJ
eurjchem-1434	20	15	,	,	PUNCT
eurjchem-1434	20	16	selective	selective	ADJ
eurjchem-1434	20	17	and	and	CCONJ
eurjchem-1434	20	18	rapid	rapid	ADJ
eurjchem-1434	20	19	uplc‐ms	uplc‐ms	NOUN
eurjchem-1434	20	20	/	/	SYM
eurjchem-1434	20	21	ms	ms	NOUN
eurjchem-1434	20	22	method	method	NOUN
eurjchem-1434	20	23	for	for	ADP
eurjchem-1434	20	24	the	the	DET
eurjchem-1434	20	25	simultaneous	simultaneous	ADJ
eurjchem-1434	20	26	analysis	analysis	NOUN
eurjchem-1434	20	27	of	of	ADP
eurjchem-1434	20	28	the	the	DET
eurjchem-1434	20	29	cited	cite	VERB
eurjchem-1434	20	30	drug	drug	NOUN
eurjchem-1434	20	31	in	in	ADP
eurjchem-1434	20	32	pure	pure	ADJ
eurjchem-1434	20	33	form	form	NOUN
eurjchem-1434	20	34	and	and	CCONJ
eurjchem-1434	20	35	pharmaceutical	pharmaceutical	NOUN
eurjchem-1434	20	36	dosage	dosage	NOUN
eurjchem-1434	20	37	form	form	NOUN
eurjchem-1434	20	38	,	,	PUNCT
eurjchem-1434	20	39	also	also	ADV
eurjchem-1434	20	40	in	in	ADP
eurjchem-1434	20	41	presence	presence	NOUN
eurjchem-1434	20	42	of	of	ADP
eurjchem-1434	20	43	its	its	PRON
eurjchem-1434	20	44	degradation	degradation	NOUN
eurjchem-1434	20	45	products	product	NOUN
eurjchem-1434	20	46	and/or	and/or	CCONJ
eurjchem-1434	20	47	metabolite	metabolite	NOUN
eurjchem-1434	20	48	.	.	PUNCT
eurjchem-1434	21	1	different	different	ADJ
eurjchem-1434	21	2	chromato‐	chromato‐	NUM
eurjchem-1434	21	3	214	214	NUM
eurjchem-1434	21	4	abou‐el	abou‐el	ADP
eurjchem-1434	21	5	alamin	alamin	PROPN
eurjchem-1434	21	6	/	/	SYM
eurjchem-1434	21	7	european	european	PROPN
eurjchem-1434	21	8	journal	journal	PROPN
eurjchem-1434	21	9	of	of	ADP
eurjchem-1434	21	10	chemistry	chemistry	NOUN
eurjchem-1434	21	11	7	7	NUM
eurjchem-1434	21	12	(	(	PUNCT
eurjchem-1434	21	13	2	2	NUM
eurjchem-1434	21	14	)	)	PUNCT
eurjchem-1434	21	15	(	(	PUNCT
eurjchem-1434	21	16	2016	2016	NUM
eurjchem-1434	21	17	)	)	PUNCT
eurjchem-1434	21	18	213‐216	213‐216	NUM
eurjchem-1434	21	19	graphic	graphic	ADJ
eurjchem-1434	21	20	parameters	parameter	NOUN
eurjchem-1434	21	21	and	and	CCONJ
eurjchem-1434	21	22	mass	mass	ADJ
eurjchem-1434	21	23	spectrometric	spectrometric	ADJ
eurjchem-1434	21	24	conditions	condition	NOUN
eurjchem-1434	21	25	were	be	AUX
eurjchem-1434	21	26	investigated	investigate	VERB
eurjchem-1434	21	27	to	to	PART
eurjchem-1434	21	28	select	select	VERB
eurjchem-1434	21	29	the	the	DET
eurjchem-1434	21	30	optimum	optimum	ADJ
eurjchem-1434	21	31	conditions	condition	NOUN
eurjchem-1434	21	32	for	for	ADP
eurjchem-1434	21	33	the	the	DET
eurjchem-1434	21	34	separation	separation	NOUN
eurjchem-1434	21	35	.	.	PUNCT
eurjchem-1434	22	1	this	this	DET
eurjchem-1434	22	2	technique	technique	NOUN
eurjchem-1434	22	3	couples	couple	NOUN
eurjchem-1434	22	4	high	high	ADJ
eurjchem-1434	22	5	resolution	resolution	NOUN
eurjchem-1434	22	6	chromato‐	chromato‐	NOUN
eurjchem-1434	22	7	graphic	graphic	ADJ
eurjchem-1434	22	8	separation	separation	NOUN
eurjchem-1434	22	9	with	with	ADP
eurjchem-1434	22	10	sensitive	sensitive	ADJ
eurjchem-1434	22	11	and	and	CCONJ
eurjchem-1434	22	12	specific	specific	ADJ
eurjchem-1434	22	13	mass	mass	ADJ
eurjchem-1434	22	14	spectrometric	spectrometric	ADJ
eurjchem-1434	22	15	detection	detection	NOUN
eurjchem-1434	22	16	,	,	PUNCT
eurjchem-1434	22	17	which	which	PRON
eurjchem-1434	22	18	is	be	AUX
eurjchem-1434	22	19	clearly	clearly	ADV
eurjchem-1434	22	20	advantageous	advantageous	ADJ
eurjchem-1434	22	21	,	,	PUNCT
eurjchem-1434	22	22	particularly	particularly	ADV
eurjchem-1434	22	23	because	because	SCONJ
eurjchem-1434	22	24	many	many	ADJ
eurjchem-1434	22	25	compounds	compound	NOUN
eurjchem-1434	22	26	with	with	ADP
eurjchem-1434	22	27	similar	similar	ADJ
eurjchem-1434	22	28	or	or	CCONJ
eurjchem-1434	22	29	identical	identical	ADJ
eurjchem-1434	22	30	retention	retention	NOUN
eurjchem-1434	22	31	characteristics	characteristic	NOUN
eurjchem-1434	22	32	have	have	VERB
eurjchem-1434	22	33	quite	quite	ADV
eurjchem-1434	22	34	different	different	ADJ
eurjchem-1434	22	35	mass	mass	NOUN
eurjchem-1434	22	36	spectra	spectra	NOUN
eurjchem-1434	22	37	and	and	CCONJ
eurjchem-1434	22	38	can	can	AUX
eurjchem-1434	22	39	therefore	therefore	ADV
eurjchem-1434	22	40	be	be	AUX
eurjchem-1434	22	41	differentiated	differentiate	VERB
eurjchem-1434	22	42	[	[	X
eurjchem-1434	22	43	10	10	NUM
eurjchem-1434	22	44	]	]	PUNCT
eurjchem-1434	22	45	.	.	PUNCT
eurjchem-1434	23	1	2	2	X
eurjchem-1434	23	2	.	.	X
eurjchem-1434	23	3	experimental	experimental	ADJ
eurjchem-1434	23	4	2.1	2.1	NUM
eurjchem-1434	23	5	.	.	PUNCT
eurjchem-1434	23	6	materials	material	NOUN
eurjchem-1434	23	7	acemetacin	acemetacin	ADV
eurjchem-1434	23	8	(	(	PUNCT
eurjchem-1434	23	9	99.73	99.73	NUM
eurjchem-1434	23	10	%	%	NOUN
eurjchem-1434	23	11	)	)	PUNCT
eurjchem-1434	23	12	and	and	CCONJ
eurjchem-1434	23	13	indomethacin	indomethacin	X
eurjchem-1434	23	14	(	(	PUNCT
eurjchem-1434	23	15	100.36	100.36	NUM
eurjchem-1434	23	16	%	%	NOUN
eurjchem-1434	23	17	)	)	PUNCT
eurjchem-1434	23	18	were	be	AUX
eurjchem-1434	23	19	kindly	kindly	ADV
eurjchem-1434	23	20	supplied	supply	VERB
eurjchem-1434	23	21	by	by	ADP
eurjchem-1434	23	22	the	the	DET
eurjchem-1434	23	23	national	national	ADJ
eurjchem-1434	23	24	organization	organization	NOUN
eurjchem-1434	23	25	for	for	ADP
eurjchem-1434	23	26	drug	drug	NOUN
eurjchem-1434	23	27	control	control	NOUN
eurjchem-1434	23	28	and	and	CCONJ
eurjchem-1434	23	29	research	research	NOUN
eurjchem-1434	23	30	(	(	PUNCT
eurjchem-1434	23	31	nodcar	nodcar	NOUN
eurjchem-1434	23	32	)	)	PUNCT
eurjchem-1434	23	33	,	,	PUNCT
eurjchem-1434	23	34	cairo	cairo	PROPN
eurjchem-1434	23	35	,	,	PUNCT
eurjchem-1434	23	36	egypt	egypt	PROPN
eurjchem-1434	23	37	.	.	PUNCT
eurjchem-1434	24	1	pharmaceutical	pharmaceutical	ADJ
eurjchem-1434	24	2	dosage	dosage	NOUN
eurjchem-1434	24	3	forms	form	NOUN
eurjchem-1434	24	4	;	;	PUNCT
eurjchem-1434	24	5	ost‐map	ost‐map	NUM
eurjchem-1434	24	6	capsules	capsule	NOUN
eurjchem-1434	24	7	(	(	PUNCT
eurjchem-1434	24	8	60	60	NUM
eurjchem-1434	24	9	mg	mg	PROPN
eurjchem-1434	24	10	acm	acm	PROPN
eurjchem-1434	24	11	/	/	SYM
eurjchem-1434	24	12	capsule	capsule	PROPN
eurjchem-1434	24	13	)	)	PUNCT
eurjchem-1434	24	14	manufactured	manufacture	VERB
eurjchem-1434	24	15	by	by	ADP
eurjchem-1434	24	16	multi‐apex	multi‐apex	ADJ
eurjchem-1434	24	17	pharmaceutical	pharmaceutical	NOUN
eurjchem-1434	24	18	industries	industry	NOUN
eurjchem-1434	24	19	,	,	PUNCT
eurjchem-1434	24	20	badr	badr	PROPN
eurjchem-1434	24	21	city	city	PROPN
eurjchem-1434	24	22	,	,	PUNCT
eurjchem-1434	24	23	egypt	egypt	PROPN
eurjchem-1434	24	24	.	.	PUNCT
eurjchem-1434	25	1	2.2	2.2	NUM
eurjchem-1434	25	2	.	.	PUNCT
eurjchem-1434	25	3	chemicals	chemical	NOUN
eurjchem-1434	25	4	and	and	CCONJ
eurjchem-1434	25	5	reagents	reagent	NOUN
eurjchem-1434	25	6	all	all	DET
eurjchem-1434	25	7	chemicals	chemical	NOUN
eurjchem-1434	25	8	used	use	VERB
eurjchem-1434	25	9	were	be	AUX
eurjchem-1434	25	10	of	of	ADP
eurjchem-1434	25	11	analytical	analytical	ADJ
eurjchem-1434	25	12	grade	grade	NOUN
eurjchem-1434	25	13	and	and	CCONJ
eurjchem-1434	25	14	solvents	solvent	NOUN
eurjchem-1434	25	15	were	be	AUX
eurjchem-1434	25	16	of	of	ADP
eurjchem-1434	25	17	hplc	hplc	NOUN
eurjchem-1434	25	18	grade	grade	NOUN
eurjchem-1434	25	19	.	.	PUNCT
eurjchem-1434	26	1	diphenhydramine	diphenhydramine	PROPN
eurjchem-1434	26	2	(	(	PUNCT
eurjchem-1434	26	3	is	be	AUX
eurjchem-1434	26	4	)	)	PUNCT
eurjchem-1434	26	5	,	,	PUNCT
eurjchem-1434	26	6	methanol	methanol	NOUN
eurjchem-1434	26	7	,	,	PUNCT
eurjchem-1434	26	8	acetonitrile	acetonitrile	NOUN
eurjchem-1434	26	9	and	and	CCONJ
eurjchem-1434	26	10	formic	formic	PROPN
eurjchem-1434	26	11	acid	acid	PROPN
eurjchem-1434	26	12	were	be	AUX
eurjchem-1434	26	13	purchased	purchase	VERB
eurjchem-1434	26	14	from	from	ADP
eurjchem-1434	26	15	sigma‐	sigma‐	PROPN
eurjchem-1434	26	16	aldrich	aldrich	PROPN
eurjchem-1434	26	17	,	,	PUNCT
eurjchem-1434	26	18	germany	germany	PROPN
eurjchem-1434	26	19	.	.	PUNCT
eurjchem-1434	27	1	sodium	sodium	PROPN
eurjchem-1434	27	2	hydroxide	hydroxide	PROPN
eurjchem-1434	27	3	,	,	PUNCT
eurjchem-1434	27	4	hydrochloric	hydrochloric	ADJ
eurjchem-1434	27	5	acid	acid	NOUN
eurjchem-1434	27	6	(	(	PUNCT
eurjchem-1434	27	7	32	32	NUM
eurjchem-1434	27	8	%	%	NOUN
eurjchem-1434	27	9	,	,	PUNCT
eurjchem-1434	27	10	w	w	NOUN
eurjchem-1434	27	11	:	:	SYM
eurjchem-1434	27	12	v	v	NOUN
eurjchem-1434	27	13	)	)	PUNCT
eurjchem-1434	27	14	were	be	AUX
eurjchem-1434	27	15	purchased	purchase	VERB
eurjchem-1434	27	16	from	from	ADP
eurjchem-1434	27	17	el‐nasr	el‐nasr	PROPN
eurjchem-1434	27	18	company	company	NOUN
eurjchem-1434	27	19	,	,	PUNCT
eurjchem-1434	27	20	egypt	egypt	PROPN
eurjchem-1434	27	21	.	.	PUNCT
eurjchem-1434	28	1	pure	pure	ADJ
eurjchem-1434	28	2	deionized	deionize	VERB
eurjchem-1434	28	3	water	water	NOUN
eurjchem-1434	28	4	was	be	AUX
eurjchem-1434	28	5	obtained	obtain	VERB
eurjchem-1434	28	6	by	by	ADP
eurjchem-1434	28	7	elga	elga	ADJ
eurjchem-1434	28	8	labwater	labwater	NOUN
eurjchem-1434	28	9	,	,	PUNCT
eurjchem-1434	28	10	prima	prima	NOUN
eurjchem-1434	28	11	7	7	NUM
eurjchem-1434	28	12	,	,	PUNCT
eurjchem-1434	28	13	uk	uk	PROPN
eurjchem-1434	28	14	.	.	PROPN
eurjchem-1434	28	15	2.3	2.3	NUM
eurjchem-1434	28	16	.	.	PUNCT
eurjchem-1434	29	1	instrumentations	instrumentation	NOUN
eurjchem-1434	29	2	the	the	DET
eurjchem-1434	29	3	analysis	analysis	NOUN
eurjchem-1434	29	4	was	be	AUX
eurjchem-1434	29	5	achieved	achieve	VERB
eurjchem-1434	29	6	using	use	VERB
eurjchem-1434	29	7	a	a	DET
eurjchem-1434	29	8	tsq	tsq	NOUN
eurjchem-1434	29	9	quantum	quantum	NOUN
eurjchem-1434	29	10	access	access	NOUN
eurjchem-1434	29	11	max	max	PROPN
eurjchem-1434	29	12	triple	triple	ADJ
eurjchem-1434	29	13	stage	stage	NOUN
eurjchem-1434	29	14	quadrupole	quadrupole	NOUN
eurjchem-1434	29	15	mass	mass	PROPN
eurjchem-1434	29	16	spectrometer	spectrometer	NOUN
eurjchem-1434	29	17	,	,	PUNCT
eurjchem-1434	29	18	thermo	thermo	NOUN
eurjchem-1434	29	19	scientific	scientific	NOUN
eurjchem-1434	29	20	,	,	PUNCT
eurjchem-1434	29	21	new	new	PROPN
eurjchem-1434	29	22	york	york	PROPN
eurjchem-1434	29	23	,	,	PUNCT
eurjchem-1434	29	24	usa	usa	PROPN
eurjchem-1434	29	25	,	,	PUNCT
eurjchem-1434	29	26	equipped	equip	VERB
eurjchem-1434	29	27	with	with	ADP
eurjchem-1434	29	28	an	an	DET
eurjchem-1434	29	29	electrospray	electrospray	ADJ
eurjchem-1434	29	30	ionization	ionization	NOUN
eurjchem-1434	29	31	(	(	PUNCT
eurjchem-1434	29	32	esi	esi	NOUN
eurjchem-1434	29	33	)	)	PUNCT
eurjchem-1434	29	34	source	source	NOUN
eurjchem-1434	29	35	.	.	PUNCT
eurjchem-1434	30	1	the	the	DET
eurjchem-1434	30	2	control	control	NOUN
eurjchem-1434	30	3	of	of	ADP
eurjchem-1434	30	4	the	the	DET
eurjchem-1434	30	5	lc‐ms	lc‐ms	NOUN
eurjchem-1434	30	6	/	/	SYM
eurjchem-1434	30	7	ms	ms	NOUN
eurjchem-1434	30	8	system	system	NOUN
eurjchem-1434	30	9	,	,	PUNCT
eurjchem-1434	30	10	acquisition	acquisition	NOUN
eurjchem-1434	30	11	and	and	CCONJ
eurjchem-1434	30	12	analysis	analysis	NOUN
eurjchem-1434	30	13	of	of	ADP
eurjchem-1434	30	14	the	the	DET
eurjchem-1434	30	15	data	datum	NOUN
eurjchem-1434	30	16	were	be	AUX
eurjchem-1434	30	17	performed	perform	VERB
eurjchem-1434	30	18	utilizing	utilize	VERB
eurjchem-1434	30	19	xcalibur	xcalibur	PROPN
eurjchem-1434	30	20	software	software	PROPN
eurjchem-1434	30	21	version	version	PROPN
eurjchem-1434	30	22	2.2	2.2	NUM
eurjchem-1434	30	23	.	.	PUNCT
eurjchem-1434	31	1	chromatography	chromatography	NOUN
eurjchem-1434	31	2	was	be	AUX
eurjchem-1434	31	3	carried	carry	VERB
eurjchem-1434	31	4	on	on	ADP
eurjchem-1434	31	5	accela	accela	NOUN
eurjchem-1434	31	6	u‐hplc	u‐hplc	PUNCT
eurjchem-1434	31	7	system	system	NOUN
eurjchem-1434	31	8	which	which	PRON
eurjchem-1434	31	9	was	be	AUX
eurjchem-1434	31	10	composed	compose	VERB
eurjchem-1434	31	11	of	of	ADP
eurjchem-1434	31	12	accela	accela	NOUN
eurjchem-1434	31	13	1250	1250	NUM
eurjchem-1434	31	14	quaternary	quaternary	ADJ
eurjchem-1434	31	15	pump	pump	NOUN
eurjchem-1434	31	16	and	and	CCONJ
eurjchem-1434	31	17	accela	accela	NOUN
eurjchem-1434	31	18	open	open	ADJ
eurjchem-1434	31	19	autosampler	autosampler	NOUN
eurjchem-1434	31	20	,	,	PUNCT
eurjchem-1434	31	21	new	new	PROPN
eurjchem-1434	31	22	york	york	PROPN
eurjchem-1434	31	23	,	,	PUNCT
eurjchem-1434	31	24	usa	usa	PROPN
eurjchem-1434	31	25	(	(	PUNCT
eurjchem-1434	31	26	operated	operate	VERB
eurjchem-1434	31	27	at	at	ADP
eurjchem-1434	31	28	25	25	NUM
eurjchem-1434	31	29	°	°	NOUN
eurjchem-1434	31	30	c	c	NOUN
eurjchem-1434	31	31	)	)	PUNCT
eurjchem-1434	31	32	.	.	PUNCT
eurjchem-1434	32	1	2.4	2.4	NUM
eurjchem-1434	32	2	.	.	X
eurjchem-1434	32	3	chromatographic	chromatographic	ADJ
eurjchem-1434	32	4	and	and	CCONJ
eurjchem-1434	32	5	mass	mass	ADJ
eurjchem-1434	32	6	spectrometric	spectrometric	ADJ
eurjchem-1434	32	7	conditions	condition	NOUN
eurjchem-1434	32	8	chromatographic	chromatographic	ADJ
eurjchem-1434	32	9	separation	separation	NOUN
eurjchem-1434	32	10	was	be	AUX
eurjchem-1434	32	11	performed	perform	VERB
eurjchem-1434	32	12	on	on	ADP
eurjchem-1434	32	13	hypersilgold	hypersilgold	ADJ
eurjchem-1434	32	14	column	column	NOUN
eurjchem-1434	32	15	(	(	PUNCT
eurjchem-1434	32	16	c18‐bonded	c18‐bonde	VERB
eurjchem-1434	32	17	ultrapure	ultrapure	NOUN
eurjchem-1434	32	18	silica	silica	NOUN
eurjchem-1434	32	19	based	base	VERB
eurjchem-1434	32	20	column	column	NOUN
eurjchem-1434	32	21	)	)	PUNCT
eurjchem-1434	32	22	50	50	NUM
eurjchem-1434	32	23	mm	mm	NOUN
eurjchem-1434	32	24	×	×	NOUN
eurjchem-1434	32	25	2.1	2.1	NUM
eurjchem-1434	32	26	mm	mm	NOUN
eurjchem-1434	32	27	(	(	PUNCT
eurjchem-1434	32	28	1.9	1.9	NUM
eurjchem-1434	32	29	µm	µm	NOUN
eurjchem-1434	32	30	)	)	PUNCT
eurjchem-1434	32	31	preceded	precede	VERB
eurjchem-1434	32	32	by	by	ADP
eurjchem-1434	32	33	a	a	DET
eurjchem-1434	32	34	c18	c18	NOUN
eurjchem-1434	32	35	security	security	NOUN
eurjchem-1434	32	36	guard	guard	PROPN
eurjchem-1434	32	37	cartridge	cartridge	PROPN
eurjchem-1434	32	38	gemini	gemini	PROPN
eurjchem-1434	32	39	5	5	NUM
eurjchem-1434	32	40	μm	μm	NOUN
eurjchem-1434	32	41	c18	c18	NOUN
eurjchem-1434	32	42	(	(	PUNCT
eurjchem-1434	32	43	phenomenex	phenomenex	ADV
eurjchem-1434	32	44	)	)	PUNCT
eurjchem-1434	32	45	4	4	NUM
eurjchem-1434	32	46	×	×	NOUN
eurjchem-1434	32	47	3	3	NUM
eurjchem-1434	32	48	mm	mm	NOUN
eurjchem-1434	32	49	)	)	PUNCT
eurjchem-1434	32	50	.	.	PUNCT
eurjchem-1434	33	1	isocratic	isocratic	ADJ
eurjchem-1434	33	2	elution	elution	NOUN
eurjchem-1434	33	3	was	be	AUX
eurjchem-1434	33	4	achieved	achieve	VERB
eurjchem-1434	33	5	using	use	VERB
eurjchem-1434	33	6	mobile	mobile	ADJ
eurjchem-1434	33	7	phase	phase	NOUN
eurjchem-1434	33	8	consisting	consist	VERB
eurjchem-1434	33	9	of	of	ADP
eurjchem-1434	33	10	0.1	0.1	NUM
eurjchem-1434	33	11	%	%	NOUN
eurjchem-1434	33	12	formic	formic	ADJ
eurjchem-1434	33	13	acid	acid	NOUN
eurjchem-1434	33	14	aqueous	aqueous	ADJ
eurjchem-1434	33	15	solution	solution	NOUN
eurjchem-1434	33	16	and	and	CCONJ
eurjchem-1434	33	17	acetonitrile	acetonitrile	NOUN
eurjchem-1434	33	18	(	(	PUNCT
eurjchem-1434	33	19	10:90	10:90	NUM
eurjchem-1434	33	20	,	,	PUNCT
eurjchem-1434	33	21	v	v	NOUN
eurjchem-1434	33	22	:	:	PUNCT
eurjchem-1434	33	23	v	v	NOUN
eurjchem-1434	33	24	)	)	PUNCT
eurjchem-1434	33	25	and	and	CCONJ
eurjchem-1434	33	26	flow	flow	NOUN
eurjchem-1434	33	27	rate	rate	NOUN
eurjchem-1434	33	28	of	of	ADP
eurjchem-1434	33	29	250	250	NUM
eurjchem-1434	33	30	µl	µl	NOUN
eurjchem-1434	33	31	/	/	SYM
eurjchem-1434	33	32	min	min	NOUN
eurjchem-1434	33	33	,	,	PUNCT
eurjchem-1434	33	34	where	where	SCONJ
eurjchem-1434	33	35	elution	elution	NOUN
eurjchem-1434	33	36	was	be	AUX
eurjchem-1434	33	37	performed	perform	VERB
eurjchem-1434	33	38	at	at	ADP
eurjchem-1434	33	39	room	room	NOUN
eurjchem-1434	33	40	temperature	temperature	NOUN
eurjchem-1434	33	41	.	.	PUNCT
eurjchem-1434	34	1	the	the	DET
eurjchem-1434	34	2	injection	injection	NOUN
eurjchem-1434	34	3	volume	volume	NOUN
eurjchem-1434	34	4	was	be	AUX
eurjchem-1434	34	5	10	10	NUM
eurjchem-1434	34	6	µl	µl	ADP
eurjchem-1434	34	7	and	and	CCONJ
eurjchem-1434	34	8	the	the	DET
eurjchem-1434	34	9	total	total	ADJ
eurjchem-1434	34	10	run	run	NOUN
eurjchem-1434	34	11	time	time	NOUN
eurjchem-1434	34	12	for	for	ADP
eurjchem-1434	34	13	each	each	DET
eurjchem-1434	34	14	sample	sample	NOUN
eurjchem-1434	34	15	was	be	AUX
eurjchem-1434	34	16	3	3	NUM
eurjchem-1434	34	17	min	min	NOUN
eurjchem-1434	34	18	.	.	PUNCT
eurjchem-1434	35	1	the	the	DET
eurjchem-1434	35	2	mass	mass	ADJ
eurjchem-1434	35	3	spectrometric	spectrometric	ADJ
eurjchem-1434	35	4	detection	detection	NOUN
eurjchem-1434	35	5	method	method	NOUN
eurjchem-1434	35	6	was	be	AUX
eurjchem-1434	35	7	carried	carry	VERB
eurjchem-1434	35	8	out	out	ADP
eurjchem-1434	35	9	in	in	ADP
eurjchem-1434	35	10	the	the	DET
eurjchem-1434	35	11	positive‐ion	positive‐ion	NOUN
eurjchem-1434	35	12	mode	mode	NOUN
eurjchem-1434	35	13	in	in	ADP
eurjchem-1434	35	14	case	case	NOUN
eurjchem-1434	35	15	of	of	ADP
eurjchem-1434	35	16	acm	acm	PROPN
eurjchem-1434	35	17	,	,	PUNCT
eurjchem-1434	35	18	indomethacin	indomethacin	NOUN
eurjchem-1434	35	19	and	and	CCONJ
eurjchem-1434	35	20	5‐methoxy‐2‐methyl‐3‐indole	5‐methoxy‐2‐methyl‐3‐indole	NUM
eurjchem-1434	35	21	acetic	acetic	ADJ
eurjchem-1434	35	22	acid	acid	NOUN
eurjchem-1434	35	23	and	and	CCONJ
eurjchem-1434	35	24	negative	negative	ADJ
eurjchem-1434	35	25	one	one	NOUN
eurjchem-1434	35	26	for	for	ADP
eurjchem-1434	35	27	pcba	pcba	ADJ
eurjchem-1434	35	28	utilizing	utilizing	NOUN
eurjchem-1434	35	29	electrospray	electrospray	VERB
eurjchem-1434	35	30	ionization	ionization	NOUN
eurjchem-1434	35	31	(	(	PUNCT
eurjchem-1434	35	32	esi	esi	NOUN
eurjchem-1434	35	33	)	)	PUNCT
eurjchem-1434	35	34	and	and	CCONJ
eurjchem-1434	35	35	multiple	multiple	ADJ
eurjchem-1434	35	36	reactions	reaction	NOUN
eurjchem-1434	35	37	monitoring	monitor	VERB
eurjchem-1434	35	38	(	(	PUNCT
eurjchem-1434	35	39	mrm	mrm	PROPN
eurjchem-1434	35	40	)	)	PUNCT
eurjchem-1434	35	41	.	.	PUNCT
eurjchem-1434	36	1	samples	sample	NOUN
eurjchem-1434	36	2	are	be	AUX
eurjchem-1434	36	3	individually	individually	ADV
eurjchem-1434	36	4	tuned	tune	VERB
eurjchem-1434	36	5	for	for	ADP
eurjchem-1434	36	6	each	each	DET
eurjchem-1434	36	7	target	target	NOUN
eurjchem-1434	36	8	analyte	analyte	NOUN
eurjchem-1434	36	9	by	by	ADP
eurjchem-1434	36	10	direct	direct	ADJ
eurjchem-1434	36	11	injection	injection	NOUN
eurjchem-1434	36	12	of	of	ADP
eurjchem-1434	36	13	the	the	DET
eurjchem-1434	36	14	individual	individual	ADJ
eurjchem-1434	36	15	solution	solution	NOUN
eurjchem-1434	36	16	followed	follow	VERB
eurjchem-1434	36	17	by	by	ADP
eurjchem-1434	36	18	data	datum	NOUN
eurjchem-1434	36	19	acquisition	acquisition	NOUN
eurjchem-1434	36	20	and	and	CCONJ
eurjchem-1434	36	21	processing	processing	NOUN
eurjchem-1434	36	22	.	.	PUNCT
eurjchem-1434	37	1	the	the	DET
eurjchem-1434	37	2	optimized	optimize	VERB
eurjchem-1434	37	3	parameters	parameter	NOUN
eurjchem-1434	37	4	are	be	AUX
eurjchem-1434	37	5	:	:	PUNCT
eurjchem-1434	37	6	auxiliary	auxiliary	ADJ
eurjchem-1434	37	7	gas	gas	NOUN
eurjchem-1434	37	8	of	of	ADP
eurjchem-1434	37	9	2	2	NUM
eurjchem-1434	37	10	psi	psi	NOUN
eurjchem-1434	37	11	,	,	PUNCT
eurjchem-1434	37	12	sheath	sheath	NOUN
eurjchem-1434	37	13	gas	gas	NOUN
eurjchem-1434	37	14	of	of	ADP
eurjchem-1434	37	15	20	20	NUM
eurjchem-1434	37	16	psi	psi	NOUN
eurjchem-1434	37	17	,	,	PUNCT
eurjchem-1434	37	18	capillary	capillary	ADJ
eurjchem-1434	37	19	temperature	temperature	NOUN
eurjchem-1434	37	20	of	of	ADP
eurjchem-1434	37	21	270	270	NUM
eurjchem-1434	37	22	°	°	NOUN
eurjchem-1434	37	23	c	c	NOUN
eurjchem-1434	37	24	,	,	PUNCT
eurjchem-1434	37	25	turbo	turbo	NOUN
eurjchem-1434	37	26	ion	ion	NOUN
eurjchem-1434	37	27	spray	spray	VERB
eurjchem-1434	37	28	temperature	temperature	NOUN
eurjchem-1434	37	29	of	of	ADP
eurjchem-1434	37	30	400	400	NUM
eurjchem-1434	37	31	°	°	NOUN
eurjchem-1434	37	32	c	c	NOUN
eurjchem-1434	37	33	,	,	PUNCT
eurjchem-1434	37	34	capillary	capillary	ADJ
eurjchem-1434	37	35	offset	offset	NOUN
eurjchem-1434	37	36	35	35	NUM
eurjchem-1434	37	37	and	and	CCONJ
eurjchem-1434	37	38	ion	ion	NOUN
eurjchem-1434	37	39	spray	spray	NOUN
eurjchem-1434	37	40	voltage	voltage	NOUN
eurjchem-1434	37	41	of	of	ADP
eurjchem-1434	37	42	3600	3600	NUM
eurjchem-1434	37	43	v.	v.	ADP
eurjchem-1434	37	44	the	the	DET
eurjchem-1434	37	45	quadrupole	quadrupole	NOUN
eurjchem-1434	37	46	mass	mass	PROPN
eurjchem-1434	37	47	spectrometer	spectrometer	NOUN
eurjchem-1434	37	48	was	be	AUX
eurjchem-1434	37	49	operated	operate	VERB
eurjchem-1434	37	50	at	at	ADP
eurjchem-1434	37	51	the	the	DET
eurjchem-1434	37	52	mrm	mrm	PROPN
eurjchem-1434	37	53	mode	mode	NOUN
eurjchem-1434	37	54	,	,	PUNCT
eurjchem-1434	37	55	monitoring	monitor	VERB
eurjchem-1434	37	56	the	the	DET
eurjchem-1434	37	57	transition	transition	NOUN
eurjchem-1434	37	58	of	of	ADP
eurjchem-1434	37	59	molecular	molecular	ADJ
eurjchem-1434	37	60	ions	ion	NOUN
eurjchem-1434	37	61	to	to	ADP
eurjchem-1434	37	62	the	the	DET
eurjchem-1434	37	63	product	product	NOUN
eurjchem-1434	37	64	ions	ion	NOUN
eurjchem-1434	37	65	for	for	ADP
eurjchem-1434	37	66	acm	acm	PROPN
eurjchem-1434	37	67	m	m	PROPN
eurjchem-1434	37	68	/	/	SYM
eurjchem-1434	37	69	z	z	PROPN
eurjchem-1434	37	70	416.44	416.44	NUM
eurjchem-1434	37	71	→	→	SYM
eurjchem-1434	37	72	139.24	139.24	NUM
eurjchem-1434	37	73	and	and	CCONJ
eurjchem-1434	37	74	is	be	AUX
eurjchem-1434	37	75	m	m	PROPN
eurjchem-1434	37	76	/	/	SYM
eurjchem-1434	37	77	z	z	PROPN
eurjchem-1434	37	78	256.31	256.31	NUM
eurjchem-1434	37	79	→	→	SYM
eurjchem-1434	37	80	167.00	167.00	NUM
eurjchem-1434	37	81	.	.	PUNCT
eurjchem-1434	38	1	the	the	DET
eurjchem-1434	38	2	collision	collision	NOUN
eurjchem-1434	38	3	energies	energy	NOUN
eurjchem-1434	38	4	were	be	AUX
eurjchem-1434	38	5	22	22	NUM
eurjchem-1434	38	6	and	and	CCONJ
eurjchem-1434	38	7	25	25	NUM
eurjchem-1434	38	8	ev	ev	INTJ
eurjchem-1434	38	9	for	for	ADP
eurjchem-1434	38	10	acm	acm	NOUN
eurjchem-1434	38	11	and	and	CCONJ
eurjchem-1434	38	12	is	be	AUX
eurjchem-1434	38	13	,	,	PUNCT
eurjchem-1434	38	14	respectively	respectively	ADV
eurjchem-1434	38	15	.	.	PUNCT
eurjchem-1434	39	1	2.5	2.5	NUM
eurjchem-1434	39	2	.	.	PUNCT
eurjchem-1434	40	1	standard	standard	ADJ
eurjchem-1434	40	2	solutions	solution	NOUN
eurjchem-1434	40	3	standard	standard	ADJ
eurjchem-1434	40	4	stock	stock	NOUN
eurjchem-1434	40	5	solutions	solution	NOUN
eurjchem-1434	40	6	of	of	ADP
eurjchem-1434	40	7	100	100	NUM
eurjchem-1434	40	8	µg	µg	ADV
eurjchem-1434	40	9	/	/	SYM
eurjchem-1434	40	10	ml	ml	NOUN
eurjchem-1434	40	11	for	for	ADP
eurjchem-1434	40	12	acm	acm	NOUN
eurjchem-1434	40	13	and	and	CCONJ
eurjchem-1434	40	14	indomethacin	indomethacin	NOUN
eurjchem-1434	40	15	were	be	AUX
eurjchem-1434	40	16	prepared	prepare	VERB
eurjchem-1434	40	17	separately	separately	ADV
eurjchem-1434	40	18	in	in	ADP
eurjchem-1434	40	19	methanol	methanol	NOUN
eurjchem-1434	40	20	and	and	CCONJ
eurjchem-1434	40	21	stored	store	VERB
eurjchem-1434	40	22	in	in	ADP
eurjchem-1434	40	23	refrigerator	refrigerator	NOUN
eurjchem-1434	40	24	.	.	PUNCT
eurjchem-1434	41	1	sample	sample	NOUN
eurjchem-1434	41	2	degradation	degradation	NOUN
eurjchem-1434	41	3	:	:	PUNCT
eurjchem-1434	41	4	acm	acm	NOUN
eurjchem-1434	41	5	pure	pure	ADJ
eurjchem-1434	41	6	sample	sample	NOUN
eurjchem-1434	41	7	was	be	AUX
eurjchem-1434	41	8	subjected	subject	VERB
eurjchem-1434	41	9	to	to	ADP
eurjchem-1434	41	10	forced	force	VERB
eurjchem-1434	41	11	degradation	degradation	NOUN
eurjchem-1434	41	12	under	under	ADP
eurjchem-1434	41	13	different	different	ADJ
eurjchem-1434	41	14	stressed	stressed	ADJ
eurjchem-1434	41	15	conditions	condition	NOUN
eurjchem-1434	41	16	as	as	ADP
eurjchem-1434	41	17	,	,	PUNCT
eurjchem-1434	41	18	alkaline	alkaline	NOUN
eurjchem-1434	41	19	(	(	PUNCT
eurjchem-1434	41	20	0.1	0.1	NUM
eurjchem-1434	41	21	n	n	PRON
eurjchem-1434	41	22	naoh	naoh	NOUN
eurjchem-1434	41	23	for	for	ADP
eurjchem-1434	41	24	30	30	NUM
eurjchem-1434	41	25	min	min	NOUN
eurjchem-1434	41	26	at	at	ADP
eurjchem-1434	41	27	room	room	NOUN
eurjchem-1434	41	28	temperature	temperature	NOUN
eurjchem-1434	41	29	)	)	PUNCT
eurjchem-1434	41	30	or	or	CCONJ
eurjchem-1434	41	31	acidic	acidic	ADJ
eurjchem-1434	41	32	(	(	PUNCT
eurjchem-1434	41	33	reflux	reflux	NOUN
eurjchem-1434	41	34	with	with	ADP
eurjchem-1434	41	35	0.1	0.1	NUM
eurjchem-1434	41	36	n	n	PRON
eurjchem-1434	41	37	hcl	hcl	PROPN
eurjchem-1434	41	38	for	for	ADP
eurjchem-1434	41	39	3	3	NUM
eurjchem-1434	41	40	hrs	hrs	NOUN
eurjchem-1434	41	41	in	in	ADP
eurjchem-1434	41	42	boiling	boiling	NOUN
eurjchem-1434	41	43	water	water	NOUN
eurjchem-1434	41	44	bath	bath	NOUN
eurjchem-1434	41	45	)	)	PUNCT
eurjchem-1434	41	46	then	then	ADV
eurjchem-1434	41	47	neutralized	neutralize	VERB
eurjchem-1434	41	48	as	as	SCONJ
eurjchem-1434	41	49	reported	report	VERB
eurjchem-1434	41	50	[	[	X
eurjchem-1434	41	51	5	5	NUM
eurjchem-1434	41	52	]	]	PUNCT
eurjchem-1434	41	53	.	.	PUNCT
eurjchem-1434	42	1	2.6	2.6	NUM
eurjchem-1434	42	2	.	.	PUNCT
eurjchem-1434	42	3	procedures	procedure	NOUN
eurjchem-1434	42	4	2.6.1	2.6.1	NUM
eurjchem-1434	42	5	.	.	PUNCT
eurjchem-1434	43	1	calibration	calibration	NOUN
eurjchem-1434	43	2	curve	curve	NOUN
eurjchem-1434	43	3	working	work	VERB
eurjchem-1434	43	4	standard	standard	ADJ
eurjchem-1434	43	5	solutions	solution	NOUN
eurjchem-1434	43	6	of	of	ADP
eurjchem-1434	43	7	acm	acm	PROPN
eurjchem-1434	43	8	(	(	PUNCT
eurjchem-1434	43	9	8.0‐500.0	8.0‐500.0	PROPN
eurjchem-1434	43	10	ng	ng	NOUN
eurjchem-1434	43	11	/	/	SYM
eurjchem-1434	43	12	ml	ml	PROPN
eurjchem-1434	43	13	)	)	PUNCT
eurjchem-1434	43	14	were	be	AUX
eurjchem-1434	43	15	prepared	prepare	VERB
eurjchem-1434	43	16	by	by	ADP
eurjchem-1434	43	17	serial	serial	ADJ
eurjchem-1434	43	18	dilutions	dilution	NOUN
eurjchem-1434	43	19	of	of	ADP
eurjchem-1434	43	20	aliquots	aliquot	NOUN
eurjchem-1434	43	21	of	of	ADP
eurjchem-1434	43	22	the	the	DET
eurjchem-1434	43	23	standard	standard	ADJ
eurjchem-1434	43	24	stock	stock	NOUN
eurjchem-1434	43	25	solution	solution	NOUN
eurjchem-1434	43	26	with	with	ADP
eurjchem-1434	43	27	methanol	methanol	NOUN
eurjchem-1434	43	28	.	.	PUNCT
eurjchem-1434	44	1	5	5	NUM
eurjchem-1434	44	2	ng	ng	PROPN
eurjchem-1434	44	3	/	/	SYM
eurjchem-1434	44	4	ml	ml	X
eurjchem-1434	44	5	of	of	ADP
eurjchem-1434	44	6	is	be	AUX
eurjchem-1434	44	7	was	be	AUX
eurjchem-1434	44	8	added	add	VERB
eurjchem-1434	44	9	for	for	ADP
eurjchem-1434	44	10	each	each	DET
eurjchem-1434	44	11	solution	solution	NOUN
eurjchem-1434	44	12	then	then	ADV
eurjchem-1434	44	13	10	10	NUM
eurjchem-1434	44	14	μl	μl	ADP
eurjchem-1434	44	15	of	of	ADP
eurjchem-1434	44	16	each	each	DET
eurjchem-1434	44	17	solution	solution	NOUN
eurjchem-1434	44	18	was	be	AUX
eurjchem-1434	44	19	injected	inject	VERB
eurjchem-1434	44	20	into	into	ADP
eurjchem-1434	44	21	the	the	DET
eurjchem-1434	44	22	lc‐ms	lc‐ms	NOUN
eurjchem-1434	44	23	/	/	SYM
eurjchem-1434	44	24	ms	ms	NOUN
eurjchem-1434	44	25	system	system	NOUN
eurjchem-1434	44	26	.	.	PUNCT
eurjchem-1434	45	1	the	the	DET
eurjchem-1434	45	2	relative	relative	ADJ
eurjchem-1434	45	3	peak	peak	NOUN
eurjchem-1434	45	4	areas	area	NOUN
eurjchem-1434	45	5	of	of	ADP
eurjchem-1434	45	6	the	the	DET
eurjchem-1434	45	7	drug	drug	NOUN
eurjchem-1434	45	8	were	be	AUX
eurjchem-1434	45	9	plotted	plot	VERB
eurjchem-1434	45	10	versus	versus	ADP
eurjchem-1434	45	11	the	the	DET
eurjchem-1434	45	12	concentrations	concentration	NOUN
eurjchem-1434	45	13	of	of	ADP
eurjchem-1434	45	14	drug	drug	NOUN
eurjchem-1434	45	15	in	in	ADP
eurjchem-1434	45	16	ng	ng	PROPN
eurjchem-1434	45	17	/	/	SYM
eurjchem-1434	45	18	ml	ml	PROPN
eurjchem-1434	45	19	and	and	CCONJ
eurjchem-1434	45	20	the	the	DET
eurjchem-1434	45	21	corresponding	correspond	VERB
eurjchem-1434	45	22	regression	regression	NOUN
eurjchem-1434	45	23	equation	equation	NOUN
eurjchem-1434	45	24	was	be	AUX
eurjchem-1434	45	25	derived	derive	VERB
eurjchem-1434	45	26	.	.	PUNCT
eurjchem-1434	46	1	2.6.2	2.6.2	X
eurjchem-1434	46	2	.	.	PUNCT
eurjchem-1434	47	1	analysis	analysis	NOUN
eurjchem-1434	47	2	of	of	ADP
eurjchem-1434	47	3	acm	acm	PROPN
eurjchem-1434	47	4	pure	pure	ADJ
eurjchem-1434	47	5	sample	sample	NOUN
eurjchem-1434	47	6	an	an	DET
eurjchem-1434	47	7	aliquot	aliquot	NOUN
eurjchem-1434	47	8	of	of	ADP
eurjchem-1434	47	9	10	10	NUM
eurjchem-1434	47	10	µl	µl	NOUN
eurjchem-1434	47	11	of	of	ADP
eurjchem-1434	47	12	different	different	ADJ
eurjchem-1434	47	13	acm	acm	PROPN
eurjchem-1434	47	14	working	work	VERB
eurjchem-1434	47	15	standard	standard	ADJ
eurjchem-1434	47	16	solutions	solution	NOUN
eurjchem-1434	47	17	covering	cover	VERB
eurjchem-1434	47	18	the	the	DET
eurjchem-1434	47	19	concentration	concentration	NOUN
eurjchem-1434	47	20	range	range	NOUN
eurjchem-1434	47	21	(	(	PUNCT
eurjchem-1434	47	22	8.0‐500.0	8.0‐500.0	PROPN
eurjchem-1434	47	23	ng	ng	NOUN
eurjchem-1434	47	24	/	/	SYM
eurjchem-1434	47	25	ml	ml	PROPN
eurjchem-1434	47	26	)	)	PUNCT
eurjchem-1434	47	27	was	be	AUX
eurjchem-1434	47	28	injected	inject	VERB
eurjchem-1434	47	29	into	into	ADP
eurjchem-1434	47	30	uplc‐ms	uplc‐ms	ADP
eurjchem-1434	47	31	/	/	SYM
eurjchem-1434	47	32	ms	ms	NOUN
eurjchem-1434	47	33	and	and	CCONJ
eurjchem-1434	47	34	measured	measure	VERB
eurjchem-1434	47	35	by	by	ADP
eurjchem-1434	47	36	the	the	DET
eurjchem-1434	47	37	proposed	propose	VERB
eurjchem-1434	47	38	method	method	NOUN
eurjchem-1434	47	39	.	.	PUNCT
eurjchem-1434	48	1	the	the	DET
eurjchem-1434	48	2	percentage	percentage	NOUN
eurjchem-1434	48	3	recoveries	recovery	NOUN
eurjchem-1434	48	4	were	be	AUX
eurjchem-1434	48	5	calculated	calculate	VERB
eurjchem-1434	48	6	by	by	ADP
eurjchem-1434	48	7	means	mean	NOUN
eurjchem-1434	48	8	of	of	ADP
eurjchem-1434	48	9	the	the	DET
eurjchem-1434	48	10	regression	regression	NOUN
eurjchem-1434	48	11	equation	equation	NOUN
eurjchem-1434	48	12	or	or	CCONJ
eurjchem-1434	48	13	from	from	ADP
eurjchem-1434	48	14	the	the	DET
eurjchem-1434	48	15	calibration	calibration	NOUN
eurjchem-1434	48	16	graph	graph	NOUN
eurjchem-1434	48	17	.	.	PUNCT
eurjchem-1434	49	1	2.6.3	2.6.3	NUM
eurjchem-1434	49	2	.	.	PUNCT
eurjchem-1434	50	1	analysis	analysis	NOUN
eurjchem-1434	50	2	of	of	ADP
eurjchem-1434	50	3	laboratory	laboratory	NOUN
eurjchem-1434	50	4	prepared	prepare	VERB
eurjchem-1434	50	5	mixtures	mixture	NOUN
eurjchem-1434	50	6	containing	contain	VERB
eurjchem-1434	50	7	different	different	ADJ
eurjchem-1434	50	8	concentrations	concentration	NOUN
eurjchem-1434	50	9	of	of	ADP
eurjchem-1434	50	10	acm	acm	PROPN
eurjchem-1434	50	11	,	,	PUNCT
eurjchem-1434	50	12	indomethacin	indomethacin	NOUN
eurjchem-1434	50	13	and	and	CCONJ
eurjchem-1434	50	14	its	its	PRON
eurjchem-1434	50	15	degradation	degradation	NOUN
eurjchem-1434	50	16	products	product	NOUN
eurjchem-1434	50	17	aliquots	aliquot	NOUN
eurjchem-1434	50	18	of	of	ADP
eurjchem-1434	50	19	acm	acm	PROPN
eurjchem-1434	50	20	working	work	VERB
eurjchem-1434	50	21	standard	standard	ADJ
eurjchem-1434	50	22	solutions	solution	NOUN
eurjchem-1434	50	23	were	be	AUX
eurjchem-1434	50	24	mixed	mix	VERB
eurjchem-1434	50	25	with	with	ADP
eurjchem-1434	50	26	indomethacin	indomethacin	NOUN
eurjchem-1434	50	27	and	and	CCONJ
eurjchem-1434	50	28	degradation	degradation	NOUN
eurjchem-1434	50	29	products	product	NOUN
eurjchem-1434	50	30	and	and	CCONJ
eurjchem-1434	50	31	determined	determine	VERB
eurjchem-1434	50	32	by	by	ADP
eurjchem-1434	50	33	the	the	DET
eurjchem-1434	50	34	proposed	propose	VERB
eurjchem-1434	50	35	method	method	NOUN
eurjchem-1434	50	36	.	.	PUNCT
eurjchem-1434	51	1	the	the	DET
eurjchem-1434	51	2	concentrations	concentration	NOUN
eurjchem-1434	51	3	of	of	ADP
eurjchem-1434	51	4	acm	acm	PROPN
eurjchem-1434	51	5	were	be	AUX
eurjchem-1434	51	6	calculated	calculate	VERB
eurjchem-1434	51	7	from	from	ADP
eurjchem-1434	51	8	the	the	DET
eurjchem-1434	51	9	regression	regression	NOUN
eurjchem-1434	51	10	equation	equation	NOUN
eurjchem-1434	51	11	.	.	PUNCT
eurjchem-1434	52	1	2.6.4	2.6.4	NUM
eurjchem-1434	52	2	.	.	PUNCT
eurjchem-1434	53	1	analysis	analysis	NOUN
eurjchem-1434	53	2	of	of	ADP
eurjchem-1434	53	3	pharmaceutical	pharmaceutical	ADJ
eurjchem-1434	53	4	dosage	dosage	NOUN
eurjchem-1434	53	5	form	form	VERB
eurjchem-1434	53	6	the	the	DET
eurjchem-1434	53	7	contents	content	NOUN
eurjchem-1434	53	8	of	of	ADP
eurjchem-1434	53	9	ten	ten	NUM
eurjchem-1434	53	10	capsules	capsule	NOUN
eurjchem-1434	53	11	of	of	ADP
eurjchem-1434	53	12	ost‐map	ost‐map	NUM
eurjchem-1434	53	13	were	be	AUX
eurjchem-1434	53	14	weighed	weigh	VERB
eurjchem-1434	53	15	and	and	CCONJ
eurjchem-1434	53	16	mixed	mix	VERB
eurjchem-1434	53	17	well	well	ADV
eurjchem-1434	53	18	.	.	PUNCT
eurjchem-1434	54	1	an	an	DET
eurjchem-1434	54	2	accurately	accurately	ADV
eurjchem-1434	54	3	amount	amount	NOUN
eurjchem-1434	54	4	claimed	claim	VERB
eurjchem-1434	54	5	to	to	PART
eurjchem-1434	54	6	be	be	AUX
eurjchem-1434	54	7	10	10	NUM
eurjchem-1434	54	8	mg	mg	PROPN
eurjchem-1434	54	9	acm	acm	PROPN
eurjchem-1434	54	10	was	be	AUX
eurjchem-1434	54	11	mixed	mix	VERB
eurjchem-1434	54	12	with	with	ADP
eurjchem-1434	54	13	100	100	NUM
eurjchem-1434	54	14	ml	ml	NOUN
eurjchem-1434	54	15	methanol	methanol	NOUN
eurjchem-1434	54	16	then	then	ADV
eurjchem-1434	54	17	sonicated	sonicate	VERB
eurjchem-1434	54	18	for	for	ADP
eurjchem-1434	54	19	30	30	NUM
eurjchem-1434	54	20	min	min	NOUN
eurjchem-1434	54	21	.	.	PUNCT
eurjchem-1434	55	1	the	the	DET
eurjchem-1434	55	2	solution	solution	NOUN
eurjchem-1434	55	3	was	be	AUX
eurjchem-1434	55	4	filtrated	filtrate	VERB
eurjchem-1434	55	5	and	and	CCONJ
eurjchem-1434	55	6	completed	complete	VERB
eurjchem-1434	55	7	as	as	ADP
eurjchem-1434	55	8	under	under	ADP
eurjchem-1434	55	9	section	section	NOUN
eurjchem-1434	55	10	2.6.1	2.6.1	NUM
eurjchem-1434	55	11	.	.	PUNCT
eurjchem-1434	56	1	the	the	DET
eurjchem-1434	56	2	concentrations	concentration	NOUN
eurjchem-1434	56	3	of	of	ADP
eurjchem-1434	56	4	acm	acm	PROPN
eurjchem-1434	56	5	were	be	AUX
eurjchem-1434	56	6	calculated	calculate	VERB
eurjchem-1434	56	7	from	from	ADP
eurjchem-1434	56	8	the	the	DET
eurjchem-1434	56	9	corresponding	corresponding	ADJ
eurjchem-1434	56	10	regression	regression	NOUN
eurjchem-1434	56	11	equation	equation	NOUN
eurjchem-1434	56	12	.	.	PUNCT
eurjchem-1434	57	1	3	3	X
eurjchem-1434	57	2	.	.	NOUN
eurjchem-1434	57	3	results	result	NOUN
eurjchem-1434	57	4	and	and	CCONJ
eurjchem-1434	57	5	discussion	discussion	NOUN
eurjchem-1434	57	6	the	the	DET
eurjchem-1434	57	7	proposed	propose	VERB
eurjchem-1434	57	8	uplc‐ms	uplc‐ms	NOUN
eurjchem-1434	57	9	/	/	SYM
eurjchem-1434	57	10	ms	ms	PROPN
eurjchem-1434	57	11	method	method	NOUN
eurjchem-1434	57	12	permits	permit	VERB
eurjchem-1434	57	13	the	the	DET
eurjchem-1434	57	14	quantification	quantification	NOUN
eurjchem-1434	57	15	of	of	ADP
eurjchem-1434	57	16	acm	acm	NOUN
eurjchem-1434	57	17	in	in	ADP
eurjchem-1434	57	18	pure	pure	ADJ
eurjchem-1434	57	19	material	material	NOUN
eurjchem-1434	57	20	and	and	CCONJ
eurjchem-1434	57	21	in	in	ADP
eurjchem-1434	57	22	presence	presence	NOUN
eurjchem-1434	57	23	of	of	ADP
eurjchem-1434	57	24	its	its	PRON
eurjchem-1434	57	25	metabolite	metabolite	NOUN
eurjchem-1434	57	26	(	(	PUNCT
eurjchem-1434	57	27	indomethacin	indomethacin	PROPN
eurjchem-1434	57	28	)	)	PUNCT
eurjchem-1434	57	29	and	and	CCONJ
eurjchem-1434	57	30	two	two	NUM
eurjchem-1434	57	31	degradation	degradation	NOUN
eurjchem-1434	57	32	products	product	NOUN
eurjchem-1434	57	33	.	.	PUNCT
eurjchem-1434	58	1	the	the	DET
eurjchem-1434	58	2	method	method	NOUN
eurjchem-1434	58	3	suggests	suggest	VERB
eurjchem-1434	58	4	high	high	ADJ
eurjchem-1434	58	5	sensitivity	sensitivity	NOUN
eurjchem-1434	58	6	and	and	CCONJ
eurjchem-1434	58	7	selectivity	selectivity	NOUN
eurjchem-1434	58	8	for	for	ADP
eurjchem-1434	58	9	acm	acm	PROPN
eurjchem-1434	58	10	.	.	PUNCT
eurjchem-1434	59	1	3.1	3.1	NUM
eurjchem-1434	59	2	.	.	PUNCT
eurjchem-1434	59	3	selection	selection	NOUN
eurjchem-1434	59	4	and	and	CCONJ
eurjchem-1434	59	5	optimization	optimization	NOUN
eurjchem-1434	59	6	of	of	ADP
eurjchem-1434	59	7	chromatographic	chromatographic	ADJ
eurjchem-1434	59	8	condition	condition	NOUN
eurjchem-1434	59	9	and	and	CCONJ
eurjchem-1434	59	10	mass	mass	ADJ
eurjchem-1434	59	11	spectrometric	spectrometric	ADJ
eurjchem-1434	59	12	detection	detection	NOUN
eurjchem-1434	59	13	to	to	PART
eurjchem-1434	59	14	achieve	achieve	VERB
eurjchem-1434	59	15	the	the	DET
eurjchem-1434	59	16	best	good	ADJ
eurjchem-1434	59	17	chromatographic	chromatographic	ADJ
eurjchem-1434	59	18	conditions	condition	NOUN
eurjchem-1434	59	19	:	:	PUNCT
eurjchem-1434	59	20	mobile	mobile	ADJ
eurjchem-1434	59	21	phase	phase	NOUN
eurjchem-1434	59	22	composition	composition	NOUN
eurjchem-1434	59	23	and	and	CCONJ
eurjchem-1434	59	24	flow	flow	NOUN
eurjchem-1434	59	25	rate	rate	NOUN
eurjchem-1434	59	26	were	be	AUX
eurjchem-1434	59	27	carefully	carefully	ADV
eurjchem-1434	59	28	studied	study	VERB
eurjchem-1434	59	29	and	and	CCONJ
eurjchem-1434	59	30	optimized	optimize	VERB
eurjchem-1434	59	31	to	to	PART
eurjchem-1434	59	32	provide	provide	VERB
eurjchem-1434	59	33	sufficient	sufficient	ADJ
eurjchem-1434	59	34	selectivity	selectivity	NOUN
eurjchem-1434	59	35	and	and	CCONJ
eurjchem-1434	59	36	sensitivity	sensitivity	NOUN
eurjchem-1434	59	37	in	in	ADP
eurjchem-1434	59	38	a	a	DET
eurjchem-1434	59	39	short	short	ADJ
eurjchem-1434	59	40	separation	separation	NOUN
eurjchem-1434	59	41	time	time	NOUN
eurjchem-1434	59	42	.	.	PUNCT
eurjchem-1434	60	1	so	so	ADV
eurjchem-1434	60	2	,	,	PUNCT
eurjchem-1434	60	3	isocratic	isocratic	ADJ
eurjchem-1434	60	4	elution	elution	NOUN
eurjchem-1434	60	5	using	use	VERB
eurjchem-1434	60	6	mobile	mobile	ADJ
eurjchem-1434	60	7	phase	phase	NOUN
eurjchem-1434	60	8	consisting	consist	VERB
eurjchem-1434	60	9	of	of	ADP
eurjchem-1434	60	10	0.1	0.1	NUM
eurjchem-1434	60	11	%	%	NOUN
eurjchem-1434	60	12	formic	formic	ADJ
eurjchem-1434	60	13	acid	acid	NOUN
eurjchem-1434	60	14	aqueous	aqueous	ADJ
eurjchem-1434	60	15	solution	solution	NOUN
eurjchem-1434	60	16	and	and	CCONJ
eurjchem-1434	60	17	acetonitrile	acetonitrile	NOUN
eurjchem-1434	60	18	(	(	PUNCT
eurjchem-1434	60	19	10:90	10:90	NUM
eurjchem-1434	60	20	,	,	PUNCT
eurjchem-1434	60	21	v	v	NOUN
eurjchem-1434	60	22	:	:	PUNCT
eurjchem-1434	60	23	v	v	NOUN
eurjchem-1434	60	24	)	)	PUNCT
eurjchem-1434	60	25	,	,	PUNCT
eurjchem-1434	60	26	flow	flow	NOUN
eurjchem-1434	60	27	rate	rate	NOUN
eurjchem-1434	60	28	of	of	ADP
eurjchem-1434	60	29	250	250	NUM
eurjchem-1434	60	30	µl	µl	NOUN
eurjchem-1434	60	31	/	/	SYM
eurjchem-1434	60	32	min	min	NOUN
eurjchem-1434	60	33	and	and	CCONJ
eurjchem-1434	60	34	injection	injection	NOUN
eurjchem-1434	60	35	volume	volume	NOUN
eurjchem-1434	60	36	10	10	NUM
eurjchem-1434	60	37	µl	µl	ADP
eurjchem-1434	60	38	,	,	PUNCT
eurjchem-1434	60	39	performed	perform	VERB
eurjchem-1434	60	40	at	at	ADP
eurjchem-1434	60	41	room	room	NOUN
eurjchem-1434	60	42	temperature	temperature	NOUN
eurjchem-1434	60	43	allowed	allow	VERB
eurjchem-1434	60	44	high	high	ADJ
eurjchem-1434	60	45	resolution	resolution	NOUN
eurjchem-1434	60	46	and	and	CCONJ
eurjchem-1434	60	47	separation	separation	NOUN
eurjchem-1434	60	48	of	of	ADP
eurjchem-1434	60	49	each	each	DET
eurjchem-1434	60	50	analyt	analyt	ADJ
eurjchem-1434	60	51	(	(	PUNCT
eurjchem-1434	60	52	acm	acm	PROPN
eurjchem-1434	60	53	,	,	PUNCT
eurjchem-1434	60	54	indomethacin	indomethacin	NOUN
eurjchem-1434	60	55	,	,	PUNCT
eurjchem-1434	60	56	degradates	degradate	NOUN
eurjchem-1434	60	57	and	and	CCONJ
eurjchem-1434	60	58	is	be	AUX
eurjchem-1434	60	59	)	)	PUNCT
eurjchem-1434	60	60	.	.	PUNCT
eurjchem-1434	61	1	for	for	ADP
eurjchem-1434	61	2	mass	mass	ADJ
eurjchem-1434	61	3	spectrometry	spectrometry	NOUN
eurjchem-1434	61	4	,	,	PUNCT
eurjchem-1434	61	5	different	different	ADJ
eurjchem-1434	61	6	parameters	parameter	NOUN
eurjchem-1434	61	7	were	be	AUX
eurjchem-1434	61	8	studied	study	VERB
eurjchem-1434	61	9	as	as	ADP
eurjchem-1434	61	10	,	,	PUNCT
eurjchem-1434	61	11	sheath	sheath	NOUN
eurjchem-1434	61	12	gas	gas	NOUN
eurjchem-1434	61	13	pressure	pressure	NOUN
eurjchem-1434	61	14	,	,	PUNCT
eurjchem-1434	61	15	spray	spray	NOUN
eurjchem-1434	61	16	voltage	voltage	NOUN
eurjchem-1434	61	17	,	,	PUNCT
eurjchem-1434	61	18	collision	collision	NOUN
eurjchem-1434	61	19	energy	energy	NOUN
eurjchem-1434	61	20	,	,	PUNCT
eurjchem-1434	61	21	rate	rate	NOUN
eurjchem-1434	61	22	of	of	ADP
eurjchem-1434	61	23	fragmentation	fragmentation	NOUN
eurjchem-1434	61	24	,	,	PUNCT
eurjchem-1434	61	25	mode	mode	NOUN
eurjchem-1434	61	26	of	of	ADP
eurjchem-1434	61	27	ionization	ionization	NOUN
eurjchem-1434	61	28	,	,	PUNCT
eurjchem-1434	61	29	etc	etc	X
eurjchem-1434	61	30	.	.	X
eurjchem-1434	62	1	the	the	DET
eurjchem-1434	62	2	selected	select	VERB
eurjchem-1434	62	3	conditions	condition	NOUN
eurjchem-1434	62	4	(	(	PUNCT
eurjchem-1434	62	5	under	under	ADP
eurjchem-1434	62	6	section	section	NOUN
eurjchem-1434	62	7	2.4	2.4	NUM
eurjchem-1434	62	8	)	)	PUNCT
eurjchem-1434	62	9	permitted	permit	VERB
eurjchem-1434	62	10	good	good	ADJ
eurjchem-1434	62	11	separation	separation	NOUN
eurjchem-1434	62	12	in	in	ADP
eurjchem-1434	62	13	short	short	ADJ
eurjchem-1434	62	14	time	time	NOUN
eurjchem-1434	62	15	(	(	PUNCT
eurjchem-1434	62	16	less	less	ADJ
eurjchem-1434	62	17	than	than	ADP
eurjchem-1434	62	18	1	1	NUM
eurjchem-1434	62	19	min	min	NOUN
eurjchem-1434	62	20	)	)	PUNCT
eurjchem-1434	62	21	.	.	PUNCT
eurjchem-1434	63	1	the	the	DET
eurjchem-1434	63	2	optimized	optimize	VERB
eurjchem-1434	63	3	mrm	mrm	PROPN
eurjchem-1434	63	4	transitions	transition	NOUN
eurjchem-1434	63	5	(	(	PUNCT
eurjchem-1434	63	6	precursor	precursor	NOUN
eurjchem-1434	63	7	ion	ion	NOUN
eurjchem-1434	63	8	m	m	PROPN
eurjchem-1434	63	9	/	/	SYM
eurjchem-1434	63	10	z	z	NOUN
eurjchem-1434	63	11	→	→	SYM
eurjchem-1434	63	12	product	product	NOUN
eurjchem-1434	63	13	ion	ion	NOUN
eurjchem-1434	63	14	m	m	PROPN
eurjchem-1434	63	15	/	/	SYM
eurjchem-1434	63	16	z	z	NOUN
eurjchem-1434	63	17	)	)	PUNCT
eurjchem-1434	63	18	are	be	AUX
eurjchem-1434	63	19	acm	acm	PROPN
eurjchem-1434	63	20	m	m	PROPN
eurjchem-1434	63	21	/	/	SYM
eurjchem-1434	63	22	z	z	PROPN
eurjchem-1434	63	23	416.44	416.44	NUM
eurjchem-1434	63	24	→	→	SYM
eurjchem-1434	63	25	139.24	139.24	NUM
eurjchem-1434	63	26	and	and	CCONJ
eurjchem-1434	63	27	is	be	AUX
eurjchem-1434	63	28	m	m	PROPN
eurjchem-1434	63	29	/	/	SYM
eurjchem-1434	63	30	z	z	PROPN
eurjchem-1434	63	31	256.31	256.31	NUM
eurjchem-1434	63	32	→	→	SYM
eurjchem-1434	63	33	167.00	167.00	NUM
eurjchem-1434	63	34	,	,	PUNCT
eurjchem-1434	63	35	where	where	SCONJ
eurjchem-1434	63	36	,	,	PUNCT
eurjchem-1434	63	37	full	full	ADJ
eurjchem-1434	63	38	scan	scan	NOUN
eurjchem-1434	63	39	for	for	ADP
eurjchem-1434	63	40	pcba	pcba	NOUN
eurjchem-1434	63	41	m	m	PROPN
eurjchem-1434	63	42	/	/	SYM
eurjchem-1434	63	43	z	z	PROPN
eurjchem-1434	63	44	156.32	156.32	NUM
eurjchem-1434	63	45	→	→	SYM
eurjchem-1434	63	46	156.32	156.32	NUM
eurjchem-1434	63	47	,	,	PUNCT
eurjchem-1434	63	48	5‐methoxy‐2‐methyl‐3‐indole	5‐methoxy‐2‐methyl‐3‐indole	NUM
eurjchem-1434	63	49	acetic	acetic	ADJ
eurjchem-1434	63	50	acid	acid	NOUN
eurjchem-1434	63	51	abou‐el	abou‐el	PROPN
eurjchem-1434	63	52	alamin	alamin	PROPN
eurjchem-1434	63	53	/	/	SYM
eurjchem-1434	63	54	european	european	PROPN
eurjchem-1434	63	55	journal	journal	PROPN
eurjchem-1434	63	56	of	of	ADP
eurjchem-1434	63	57	chemistry	chemistry	NOUN
eurjchem-1434	63	58	7	7	NUM
eurjchem-1434	63	59	(	(	PUNCT
eurjchem-1434	63	60	2	2	NUM
eurjchem-1434	63	61	)	)	PUNCT
eurjchem-1434	63	62	(	(	PUNCT
eurjchem-1434	63	63	2016	2016	NUM
eurjchem-1434	63	64	)	)	PUNCT
eurjchem-1434	63	65	213‐216	213‐216	NUM
eurjchem-1434	63	66	215	215	NUM
eurjchem-1434	63	67	m	m	NOUN
eurjchem-1434	63	68	/	/	SYM
eurjchem-1434	63	69	z	z	PROPN
eurjchem-1434	63	70	220.30	220.30	NUM
eurjchem-1434	63	71	→	→	SYM
eurjchem-1434	63	72	220.30	220.30	NUM
eurjchem-1434	63	73	and	and	CCONJ
eurjchem-1434	63	74	indomethacin	indomethacin	VERB
eurjchem-1434	63	75	m	m	PROPN
eurjchem-1434	63	76	/	/	SYM
eurjchem-1434	63	77	z	z	NOUN
eurjchem-1434	63	78	358.35	358.35	NUM
eurjchem-1434	63	79	→	→	SYM
eurjchem-1434	63	80	358.35	358.35	NUM
eurjchem-1434	63	81	(	(	PUNCT
eurjchem-1434	63	82	figure	figure	NOUN
eurjchem-1434	63	83	2	2	NUM
eurjchem-1434	63	84	)	)	PUNCT
eurjchem-1434	63	85	.	.	PUNCT
eurjchem-1434	64	1	acm	acm	PROPN
eurjchem-1434	64	2	was	be	AUX
eurjchem-1434	64	3	fragmented	fragment	VERB
eurjchem-1434	64	4	into	into	ADP
eurjchem-1434	64	5	different	different	ADJ
eurjchem-1434	64	6	product	product	NOUN
eurjchem-1434	64	7	ions	ion	NOUN
eurjchem-1434	64	8	m	m	PROPN
eurjchem-1434	64	9	/	/	SYM
eurjchem-1434	64	10	z	z	PROPN
eurjchem-1434	64	11	139.24	139.24	NUM
eurjchem-1434	64	12	,	,	PUNCT
eurjchem-1434	64	13	111.28	111.28	NUM
eurjchem-1434	64	14	and	and	CCONJ
eurjchem-1434	64	15	174.30	174.30	NUM
eurjchem-1434	64	16	,	,	PUNCT
eurjchem-1434	64	17	but	but	CCONJ
eurjchem-1434	64	18	we	we	PRON
eurjchem-1434	64	19	selected	select	VERB
eurjchem-1434	64	20	139.24	139.24	NUM
eurjchem-1434	64	21	because	because	SCONJ
eurjchem-1434	64	22	it	it	PRON
eurjchem-1434	64	23	gave	give	VERB
eurjchem-1434	64	24	high	high	ADJ
eurjchem-1434	64	25	intensity	intensity	NOUN
eurjchem-1434	64	26	(	(	PUNCT
eurjchem-1434	64	27	figure	figure	NOUN
eurjchem-1434	64	28	3	3	NUM
eurjchem-1434	64	29	and	and	CCONJ
eurjchem-1434	64	30	4	4	NUM
eurjchem-1434	64	31	)	)	PUNCT
eurjchem-1434	64	32	.	.	PUNCT
eurjchem-1434	65	1	figure	figure	NOUN
eurjchem-1434	65	2	2	2	NUM
eurjchem-1434	65	3	.	.	PUNCT
eurjchem-1434	65	4	chromatographic	chromatographic	ADJ
eurjchem-1434	65	5	separation	separation	NOUN
eurjchem-1434	65	6	of	of	ADP
eurjchem-1434	65	7	pcba	pcba	NOUN
eurjchem-1434	65	8	,	,	PUNCT
eurjchem-1434	65	9	5‐methoxy‐2‐	5‐methoxy‐2‐	NUM
eurjchem-1434	65	10	methyl	methyl	NOUN
eurjchem-1434	65	11	‐3‐indole	‐3‐indole	NOUN
eurjchem-1434	65	12	acetic	acetic	ADJ
eurjchem-1434	65	13	acid	acid	NOUN
eurjchem-1434	65	14	,	,	PUNCT
eurjchem-1434	65	15	indomethacin	indomethacin	NOUN
eurjchem-1434	65	16	and	and	CCONJ
eurjchem-1434	65	17	acm	acm	PROPN
eurjchem-1434	65	18	,	,	PUNCT
eurjchem-1434	65	19	respectively	respectively	ADV
eurjchem-1434	65	20	,	,	PUNCT
eurjchem-1434	65	21	by	by	ADP
eurjchem-1434	65	22	the	the	DET
eurjchem-1434	65	23	proposed	propose	VERB
eurjchem-1434	65	24	uplc‐ms	uplc‐ms	NOUN
eurjchem-1434	65	25	/	/	SYM
eurjchem-1434	65	26	ms	ms	PROPN
eurjchem-1434	65	27	.	.	PROPN
eurjchem-1434	65	28	figure	figure	PROPN
eurjchem-1434	65	29	3	3	NUM
eurjchem-1434	65	30	.	.	PUNCT
eurjchem-1434	65	31	breakdown	breakdown	ADJ
eurjchem-1434	65	32	curve	curve	NOUN
eurjchem-1434	65	33	of	of	ADP
eurjchem-1434	65	34	acm	acm	PROPN
eurjchem-1434	65	35	m	m	PROPN
eurjchem-1434	65	36	/	/	SYM
eurjchem-1434	65	37	z	z	PROPN
eurjchem-1434	65	38	416.44	416.44	NUM
eurjchem-1434	65	39	→	→	SYM
eurjchem-1434	65	40	139.24	139.24	NUM
eurjchem-1434	65	41	,	,	PUNCT
eurjchem-1434	65	42	111.3	111.3	NUM
eurjchem-1434	65	43	and	and	CCONJ
eurjchem-1434	65	44	174.3	174.3	NUM
eurjchem-1434	65	45	.	.	PUNCT
eurjchem-1434	66	1	figure	figure	NOUN
eurjchem-1434	66	2	4	4	NUM
eurjchem-1434	66	3	.	.	PUNCT
eurjchem-1434	66	4	product	product	NOUN
eurjchem-1434	66	5	ion	ion	NOUN
eurjchem-1434	66	6	spectra	spectra	NOUN
eurjchem-1434	66	7	of	of	ADP
eurjchem-1434	66	8	acm	acm	PROPN
eurjchem-1434	66	9	[	[	X
eurjchem-1434	66	10	m+h]+	m+h]+	PROPN
eurjchem-1434	66	11	,	,	PUNCT
eurjchem-1434	66	12	m	m	PROPN
eurjchem-1434	66	13	/	/	SYM
eurjchem-1434	66	14	z	z	PROPN
eurjchem-1434	66	15	139.2	139.2	NUM
eurjchem-1434	66	16	,	,	PUNCT
eurjchem-1434	66	17	111.3	111.3	NUM
eurjchem-1434	66	18	and	and	CCONJ
eurjchem-1434	66	19	174.3	174.3	NUM
eurjchem-1434	66	20	.	.	NOUN
eurjchem-1434	66	21	3.2	3.2	NUM
eurjchem-1434	66	22	.	.	PUNCT
eurjchem-1434	67	1	degradation	degradation	NOUN
eurjchem-1434	67	2	acm	acm	PROPN
eurjchem-1434	67	3	under	under	ADP
eurjchem-1434	67	4	different	different	ADJ
eurjchem-1434	67	5	stressed	stressed	ADJ
eurjchem-1434	67	6	acidic	acidic	ADJ
eurjchem-1434	67	7	(	(	PUNCT
eurjchem-1434	67	8	reflux	reflux	NOUN
eurjchem-1434	67	9	with	with	ADP
eurjchem-1434	67	10	0.1	0.1	NUM
eurjchem-1434	67	11	n	n	PRON
eurjchem-1434	67	12	hcl	hcl	PROPN
eurjchem-1434	67	13	for	for	ADP
eurjchem-1434	67	14	3	3	NUM
eurjchem-1434	67	15	hrs	hrs	NOUN
eurjchem-1434	67	16	in	in	ADP
eurjchem-1434	67	17	boiling	boiling	NOUN
eurjchem-1434	67	18	water	water	NOUN
eurjchem-1434	67	19	bath	bath	NOUN
eurjchem-1434	67	20	)	)	PUNCT
eurjchem-1434	67	21	and	and	CCONJ
eurjchem-1434	67	22	basic	basic	ADJ
eurjchem-1434	67	23	(	(	PUNCT
eurjchem-1434	67	24	0.1	0.1	NUM
eurjchem-1434	67	25	n	n	PRON
eurjchem-1434	67	26	naoh	naoh	NOUN
eurjchem-1434	67	27	for	for	ADP
eurjchem-1434	67	28	30	30	NUM
eurjchem-1434	67	29	min	min	NOUN
eurjchem-1434	67	30	at	at	ADP
eurjchem-1434	67	31	room	room	NOUN
eurjchem-1434	67	32	temperature	temperature	NOUN
eurjchem-1434	67	33	)	)	PUNCT
eurjchem-1434	67	34	conditions	condition	NOUN
eurjchem-1434	67	35	undergo	undergo	VERB
eurjchem-1434	67	36	complete	complete	ADJ
eurjchem-1434	67	37	degradation	degradation	NOUN
eurjchem-1434	67	38	,	,	PUNCT
eurjchem-1434	67	39	where	where	SCONJ
eurjchem-1434	67	40	it	it	PRON
eurjchem-1434	67	41	is	be	AUX
eurjchem-1434	67	42	stable	stable	ADJ
eurjchem-1434	67	43	under	under	ADP
eurjchem-1434	67	44	oxidative	oxidative	ADJ
eurjchem-1434	67	45	and	and	CCONJ
eurjchem-1434	67	46	thermal	thermal	ADJ
eurjchem-1434	67	47	stress	stress	NOUN
eurjchem-1434	67	48	conditions	condition	NOUN
eurjchem-1434	67	49	as	as	SCONJ
eurjchem-1434	67	50	reported	report	VERB
eurjchem-1434	67	51	[	[	X
eurjchem-1434	67	52	5	5	NUM
eurjchem-1434	67	53	]	]	PUNCT
eurjchem-1434	67	54	.	.	PUNCT
eurjchem-1434	68	1	acm	acm	PROPN
eurjchem-1434	68	2	was	be	AUX
eurjchem-1434	68	3	degradated	degradate	VERB
eurjchem-1434	68	4	into	into	ADP
eurjchem-1434	68	5	pcba	pcba	NOUN
eurjchem-1434	68	6	and	and	CCONJ
eurjchem-1434	68	7	5‐methoxy‐2‐methyl‐3‐indole	5‐methoxy‐2‐methyl‐3‐indole	NUM
eurjchem-1434	68	8	acetic	acetic	ADJ
eurjchem-1434	68	9	acid	acid	NOUN
eurjchem-1434	68	10	as	as	SCONJ
eurjchem-1434	68	11	reported	report	VERB
eurjchem-1434	68	12	[	[	X
eurjchem-1434	68	13	5	5	NUM
eurjchem-1434	68	14	]	]	PUNCT
eurjchem-1434	68	15	,	,	PUNCT
eurjchem-1434	68	16	which	which	PRON
eurjchem-1434	68	17	confirmed	confirm	VERB
eurjchem-1434	68	18	by	by	ADP
eurjchem-1434	68	19	their	their	PRON
eurjchem-1434	68	20	molecular	molecular	ADJ
eurjchem-1434	68	21	weights	weight	NOUN
eurjchem-1434	68	22	m	m	NOUN
eurjchem-1434	68	23	/	/	SYM
eurjchem-1434	68	24	z	z	PROPN
eurjchem-1434	68	25	156.32	156.32	NUM
eurjchem-1434	68	26	,	,	PUNCT
eurjchem-1434	68	27	220.30	220.30	NUM
eurjchem-1434	68	28	using	use	VERB
eurjchem-1434	68	29	the	the	DET
eurjchem-1434	68	30	proposed	propose	VERB
eurjchem-1434	68	31	method	method	NOUN
eurjchem-1434	68	32	(	(	PUNCT
eurjchem-1434	68	33	full	full	ADJ
eurjchem-1434	68	34	scan	scan	NOUN
eurjchem-1434	68	35	)	)	PUNCT
eurjchem-1434	68	36	.	.	PUNCT
eurjchem-1434	69	1	so	so	ADV
eurjchem-1434	69	2	,	,	PUNCT
eurjchem-1434	69	3	by	by	ADP
eurjchem-1434	69	4	applying	apply	VERB
eurjchem-1434	69	5	the	the	DET
eurjchem-1434	69	6	proposed	propose	VERB
eurjchem-1434	69	7	uplc‐ms	uplc‐ms	NOUN
eurjchem-1434	69	8	/	/	SYM
eurjchem-1434	69	9	ms	ms	NOUN
eurjchem-1434	69	10	technique	technique	NOUN
eurjchem-1434	69	11	,	,	PUNCT
eurjchem-1434	69	12	it	it	PRON
eurjchem-1434	69	13	was	be	AUX
eurjchem-1434	69	14	probable	probable	ADJ
eurjchem-1434	69	15	to	to	PART
eurjchem-1434	69	16	detect	detect	VERB
eurjchem-1434	69	17	acm	acm	NOUN
eurjchem-1434	69	18	in	in	ADP
eurjchem-1434	69	19	the	the	DET
eurjchem-1434	69	20	presence	presence	NOUN
eurjchem-1434	69	21	of	of	ADP
eurjchem-1434	69	22	its	its	PRON
eurjchem-1434	69	23	metabolite	metabolite	NOUN
eurjchem-1434	69	24	and/or	and/or	CCONJ
eurjchem-1434	69	25	degradation	degradation	NOUN
eurjchem-1434	69	26	products	product	NOUN
eurjchem-1434	69	27	in	in	ADP
eurjchem-1434	69	28	short	short	ADJ
eurjchem-1434	69	29	time	time	NOUN
eurjchem-1434	69	30	(	(	PUNCT
eurjchem-1434	69	31	˂	˂	PROPN
eurjchem-1434	69	32	1	1	NUM
eurjchem-1434	69	33	min	min	NOUN
eurjchem-1434	69	34	)	)	PUNCT
eurjchem-1434	69	35	as	as	SCONJ
eurjchem-1434	69	36	shown	show	VERB
eurjchem-1434	69	37	in	in	ADP
eurjchem-1434	69	38	figure	figure	NOUN
eurjchem-1434	69	39	2	2	NUM
eurjchem-1434	69	40	.	.	NOUN
eurjchem-1434	69	41	3.3	3.3	NUM
eurjchem-1434	69	42	.	.	PUNCT
eurjchem-1434	70	1	method	method	NOUN
eurjchem-1434	70	2	validation	validation	NOUN
eurjchem-1434	70	3	the	the	DET
eurjchem-1434	70	4	method	method	NOUN
eurjchem-1434	70	5	was	be	AUX
eurjchem-1434	70	6	validated	validate	VERB
eurjchem-1434	70	7	according	accord	VERB
eurjchem-1434	70	8	to	to	ADP
eurjchem-1434	70	9	ich	ich	NOUN
eurjchem-1434	70	10	guidelines	guideline	NOUN
eurjchem-1434	70	11	regarding	regard	VERB
eurjchem-1434	70	12	linearity	linearity	NOUN
eurjchem-1434	70	13	,	,	PUNCT
eurjchem-1434	70	14	range	range	NOUN
eurjchem-1434	70	15	,	,	PUNCT
eurjchem-1434	70	16	limit	limit	NOUN
eurjchem-1434	70	17	of	of	ADP
eurjchem-1434	70	18	detection	detection	NOUN
eurjchem-1434	70	19	,	,	PUNCT
eurjchem-1434	70	20	limit	limit	NOUN
eurjchem-1434	70	21	of	of	ADP
eurjchem-1434	70	22	quantification	quantification	NOUN
eurjchem-1434	70	23	,	,	PUNCT
eurjchem-1434	70	24	accuracy	accuracy	NOUN
eurjchem-1434	70	25	and	and	CCONJ
eurjchem-1434	70	26	precision	precision	NOUN
eurjchem-1434	70	27	[	[	X
eurjchem-1434	70	28	11	11	NUM
eurjchem-1434	70	29	]	]	PUNCT
eurjchem-1434	70	30	.	.	PUNCT
eurjchem-1434	71	1	3.3.1	3.3.1	X
eurjchem-1434	71	2	.	.	X
eurjchem-1434	71	3	linearity	linearity	NOUN
eurjchem-1434	71	4	and	and	CCONJ
eurjchem-1434	71	5	range	range	VERB
eurjchem-1434	71	6	under	under	ADP
eurjchem-1434	71	7	the	the	DET
eurjchem-1434	71	8	above‐described	above‐described	ADJ
eurjchem-1434	71	9	experimental	experimental	ADJ
eurjchem-1434	71	10	conditions	condition	NOUN
eurjchem-1434	71	11	,	,	PUNCT
eurjchem-1434	71	12	linear	linear	ADJ
eurjchem-1434	71	13	relationships	relationship	NOUN
eurjchem-1434	71	14	were	be	AUX
eurjchem-1434	71	15	established	establish	VERB
eurjchem-1434	71	16	by	by	ADP
eurjchem-1434	71	17	plotting	plot	VERB
eurjchem-1434	71	18	relative	relative	ADJ
eurjchem-1434	71	19	peak	peak	NOUN
eurjchem-1434	71	20	areas	area	NOUN
eurjchem-1434	71	21	against	against	ADP
eurjchem-1434	71	22	acm	acm	NOUN
eurjchem-1434	71	23	concentrations	concentration	NOUN
eurjchem-1434	71	24	.	.	PUNCT
eurjchem-1434	72	1	the	the	DET
eurjchem-1434	72	2	concentration	concentration	NOUN
eurjchem-1434	72	3	range	range	NOUN
eurjchem-1434	72	4	was	be	AUX
eurjchem-1434	72	5	found	find	VERB
eurjchem-1434	72	6	linear	linear	ADJ
eurjchem-1434	72	7	in	in	ADP
eurjchem-1434	72	8	8.0‐500.0	8.0‐500.0	ADJ
eurjchem-1434	72	9	ng	ng	PROPN
eurjchem-1434	72	10	/	/	SYM
eurjchem-1434	72	11	ml	ml	PROPN
eurjchem-1434	72	12	.	.	PUNCT
eurjchem-1434	73	1	linear	linear	PROPN
eurjchem-1434	73	2	regression	regression	NOUN
eurjchem-1434	73	3	analysis	analysis	NOUN
eurjchem-1434	73	4	of	of	ADP
eurjchem-1434	73	5	the	the	DET
eurjchem-1434	73	6	data	datum	NOUN
eurjchem-1434	73	7	gave	give	VERB
eurjchem-1434	73	8	the	the	DET
eurjchem-1434	73	9	following	follow	VERB
eurjchem-1434	73	10	equation	equation	NOUN
eurjchem-1434	73	11	(	(	PUNCT
eurjchem-1434	73	12	table	table	NOUN
eurjchem-1434	73	13	1	1	NUM
eurjchem-1434	73	14	):	):	PUNCT
eurjchem-1434	73	15	a	a	DET
eurjchem-1434	73	16	=	=	X
eurjchem-1434	73	17	‐1.044	‐1.044	ADP
eurjchem-1434	73	18	+	+	NOUN
eurjchem-1434	73	19	0.6353	0.6353	NUM
eurjchem-1434	73	20	×	×	NOUN
eurjchem-1434	73	21	c	c	NOUN
eurjchem-1434	73	22	(	(	PUNCT
eurjchem-1434	73	23	r	r	NOUN
eurjchem-1434	73	24	=	=	SYM
eurjchem-1434	73	25	0.9994	0.9994	NUM
eurjchem-1434	73	26	)	)	PUNCT
eurjchem-1434	73	27	(	(	PUNCT
eurjchem-1434	73	28	1	1	X
eurjchem-1434	73	29	)	)	PUNCT
eurjchem-1434	73	30	where	where	SCONJ
eurjchem-1434	73	31	a	a	PRON
eurjchem-1434	73	32	is	be	AUX
eurjchem-1434	73	33	the	the	DET
eurjchem-1434	73	34	relative	relative	ADJ
eurjchem-1434	73	35	peak	peak	NOUN
eurjchem-1434	73	36	areas	area	NOUN
eurjchem-1434	73	37	and	and	CCONJ
eurjchem-1434	73	38	c	c	NOUN
eurjchem-1434	73	39	is	be	AUX
eurjchem-1434	73	40	the	the	DET
eurjchem-1434	73	41	concentration	concentration	NOUN
eurjchem-1434	73	42	of	of	ADP
eurjchem-1434	73	43	drug	drug	NOUN
eurjchem-1434	73	44	in	in	ADP
eurjchem-1434	73	45	ng	ng	PROPN
eurjchem-1434	73	46	/	/	SYM
eurjchem-1434	73	47	ml	ml	PROPN
eurjchem-1434	73	48	and	and	CCONJ
eurjchem-1434	73	49	r	r	NOUN
eurjchem-1434	73	50	is	be	AUX
eurjchem-1434	73	51	the	the	DET
eurjchem-1434	73	52	regression	regression	NOUN
eurjchem-1434	73	53	coefficient	coefficient	NOUN
eurjchem-1434	73	54	.	.	PUNCT
eurjchem-1434	74	1	the	the	DET
eurjchem-1434	74	2	high	high	ADJ
eurjchem-1434	74	3	values	value	NOUN
eurjchem-1434	74	4	of	of	ADP
eurjchem-1434	74	5	the	the	DET
eurjchem-1434	74	6	correlation	correlation	NOUN
eurjchem-1434	74	7	coefficients	coefficient	NOUN
eurjchem-1434	74	8	(	(	PUNCT
eurjchem-1434	74	9	>	>	X
eurjchem-1434	74	10	0.999	0.999	NUM
eurjchem-1434	74	11	)	)	PUNCT
eurjchem-1434	74	12	indicate	indicate	VERB
eurjchem-1434	74	13	good	good	ADJ
eurjchem-1434	74	14	linearity	linearity	NOUN
eurjchem-1434	74	15	of	of	ADP
eurjchem-1434	74	16	the	the	DET
eurjchem-1434	74	17	calibration	calibration	NOUN
eurjchem-1434	74	18	graphs	graph	NOUN
eurjchem-1434	74	19	(	(	PUNCT
eurjchem-1434	74	20	figure	figure	NOUN
eurjchem-1434	74	21	5	5	NUM
eurjchem-1434	74	22	)	)	PUNCT
eurjchem-1434	74	23	figure	figure	NOUN
eurjchem-1434	74	24	5	5	NUM
eurjchem-1434	74	25	.	.	PUNCT
eurjchem-1434	74	26	calibration	calibration	NOUN
eurjchem-1434	74	27	curve	curve	NOUN
eurjchem-1434	74	28	of	of	ADP
eurjchem-1434	74	29	acm	acm	PROPN
eurjchem-1434	74	30	(	(	PUNCT
eurjchem-1434	74	31	8.0‐500.0	8.0‐500.0	PROPN
eurjchem-1434	74	32	ng	ng	NOUN
eurjchem-1434	74	33	/	/	SYM
eurjchem-1434	74	34	ml	ml	NOUN
eurjchem-1434	74	35	)	)	PUNCT
eurjchem-1434	74	36	by	by	ADP
eurjchem-1434	74	37	the	the	DET
eurjchem-1434	74	38	proposed	propose	VERB
eurjchem-1434	74	39	uplc‐ms	uplc‐ms	NOUN
eurjchem-1434	74	40	/	/	SYM
eurjchem-1434	74	41	ms	ms	NOUN
eurjchem-1434	74	42	method	method	NOUN
eurjchem-1434	74	43	.	.	PUNCT
eurjchem-1434	75	1	3.3.2	3.3.2	X
eurjchem-1434	75	2	.	.	X
eurjchem-1434	76	1	limit	limit	NOUN
eurjchem-1434	76	2	of	of	ADP
eurjchem-1434	76	3	quantitation	quantitation	NOUN
eurjchem-1434	76	4	(	(	PUNCT
eurjchem-1434	76	5	loq	loq	PROPN
eurjchem-1434	76	6	)	)	PUNCT
eurjchem-1434	76	7	and	and	CCONJ
eurjchem-1434	76	8	limit	limit	NOUN
eurjchem-1434	76	9	of	of	ADP
eurjchem-1434	76	10	detection	detection	NOUN
eurjchem-1434	76	11	(	(	PUNCT
eurjchem-1434	76	12	lod	lod	PROPN
eurjchem-1434	76	13	)	)	PUNCT
eurjchem-1434	76	14	the	the	DET
eurjchem-1434	76	15	minimum	minimum	ADJ
eurjchem-1434	76	16	level	level	NOUN
eurjchem-1434	76	17	at	at	ADP
eurjchem-1434	76	18	which	which	PRON
eurjchem-1434	76	19	the	the	DET
eurjchem-1434	76	20	acm	acm	NOUN
eurjchem-1434	76	21	can	can	AUX
eurjchem-1434	76	22	be	be	AUX
eurjchem-1434	76	23	reliably	reliably	ADV
eurjchem-1434	76	24	detected	detect	VERB
eurjchem-1434	76	25	(	(	PUNCT
eurjchem-1434	76	26	lod	lod	PROPN
eurjchem-1434	76	27	)	)	PUNCT
eurjchem-1434	76	28	and	and	CCONJ
eurjchem-1434	76	29	quantified	quantify	VERB
eurjchem-1434	76	30	(	(	PUNCT
eurjchem-1434	76	31	loq	loq	PROPN
eurjchem-1434	76	32	)	)	PUNCT
eurjchem-1434	76	33	were	be	AUX
eurjchem-1434	76	34	determined	determine	VERB
eurjchem-1434	76	35	and	and	CCONJ
eurjchem-1434	76	36	the	the	DET
eurjchem-1434	76	37	data	datum	NOUN
eurjchem-1434	76	38	are	be	AUX
eurjchem-1434	76	39	presented	present	VERB
eurjchem-1434	76	40	in	in	ADP
eurjchem-1434	76	41	table	table	NOUN
eurjchem-1434	76	42	1	1	NUM
eurjchem-1434	76	43	.	.	X
eurjchem-1434	77	1	3.3.3	3.3.3	NUM
eurjchem-1434	77	2	.	.	PUNCT
eurjchem-1434	78	1	accuracy	accuracy	NOUN
eurjchem-1434	78	2	and	and	CCONJ
eurjchem-1434	78	3	precision	precision	NOUN
eurjchem-1434	78	4	the	the	DET
eurjchem-1434	78	5	accuracy	accuracy	NOUN
eurjchem-1434	78	6	of	of	ADP
eurjchem-1434	78	7	the	the	DET
eurjchem-1434	78	8	proposed	propose	VERB
eurjchem-1434	78	9	method	method	NOUN
eurjchem-1434	78	10	was	be	AUX
eurjchem-1434	78	11	evaluated	evaluate	VERB
eurjchem-1434	78	12	by	by	ADP
eurjchem-1434	78	13	assay	assay	PROPN
eurjchem-1434	78	14	of	of	ADP
eurjchem-1434	78	15	acm	acm	PROPN
eurjchem-1434	78	16	standard	standard	ADJ
eurjchem-1434	78	17	solutions	solution	NOUN
eurjchem-1434	78	18	by	by	ADP
eurjchem-1434	78	19	the	the	DET
eurjchem-1434	78	20	proposed	propose	VERB
eurjchem-1434	78	21	method	method	NOUN
eurjchem-1434	78	22	and	and	CCONJ
eurjchem-1434	78	23	the	the	DET
eurjchem-1434	78	24	results	result	NOUN
eurjchem-1434	78	25	obtained	obtain	VERB
eurjchem-1434	78	26	were	be	AUX
eurjchem-1434	78	27	compared	compare	VERB
eurjchem-1434	78	28	with	with	ADP
eurjchem-1434	78	29	those	those	PRON
eurjchem-1434	78	30	obtained	obtain	VERB
eurjchem-1434	78	31	using	use	VERB
eurjchem-1434	78	32	the	the	DET
eurjchem-1434	78	33	reported	report	VERB
eurjchem-1434	78	34	one	one	NUM
eurjchem-1434	78	35	[	[	X
eurjchem-1434	78	36	5	5	NUM
eurjchem-1434	78	37	]	]	PUNCT
eurjchem-1434	78	38	.	.	PUNCT
eurjchem-1434	79	1	statistical	statistical	ADJ
eurjchem-1434	79	2	analysis	analysis	NOUN
eurjchem-1434	79	3	of	of	ADP
eurjchem-1434	79	4	the	the	DET
eurjchem-1434	79	5	results	result	NOUN
eurjchem-1434	79	6	obtained	obtain	VERB
eurjchem-1434	79	7	by	by	ADP
eurjchem-1434	79	8	the	the	DET
eurjchem-1434	79	9	proposed	propose	VERB
eurjchem-1434	79	10	and	and	CCONJ
eurjchem-1434	79	11	reported	report	VERB
eurjchem-1434	79	12	methods	method	NOUN
eurjchem-1434	79	13	using	use	VERB
eurjchem-1434	79	14	student´s	student´s	NOUN
eurjchem-1434	79	15	t‐test	t‐test	PUNCT
eurjchem-1434	79	16	and	and	CCONJ
eurjchem-1434	79	17	variance	variance	NOUN
eurjchem-1434	79	18	ratio	ratio	NOUN
eurjchem-1434	79	19	f‐test	f‐test	PUNCT
eurjchem-1434	79	20	,	,	PUNCT
eurjchem-1434	79	21	showed	show	VERB
eurjchem-1434	79	22	no	no	DET
eurjchem-1434	79	23	significant	significant	ADJ
eurjchem-1434	79	24	difference	difference	NOUN
eurjchem-1434	79	25	between	between	ADP
eurjchem-1434	79	26	the	the	DET
eurjchem-1434	79	27	two	two	NUM
eurjchem-1434	79	28	methods	method	NOUN
eurjchem-1434	79	29	(	(	PUNCT
eurjchem-1434	79	30	table	table	NOUN
eurjchem-1434	79	31	2	2	NUM
eurjchem-1434	79	32	)	)	PUNCT
eurjchem-1434	79	33	.	.	PUNCT
eurjchem-1434	80	1	evaluation	evaluation	NOUN
eurjchem-1434	80	2	of	of	ADP
eurjchem-1434	80	3	the	the	DET
eurjchem-1434	80	4	intra‐day	intra‐day	NOUN
eurjchem-1434	80	5	precision	precision	NOUN
eurjchem-1434	80	6	was	be	AUX
eurjchem-1434	80	7	made	make	VERB
eurjchem-1434	80	8	by	by	ADP
eurjchem-1434	80	9	replicate	replicate	VERB
eurjchem-1434	80	10	assay	assay	NOUN
eurjchem-1434	80	11	of	of	ADP
eurjchem-1434	80	12	the	the	DET
eurjchem-1434	80	13	standard	standard	ADJ
eurjchem-1434	80	14	solutions	solution	NOUN
eurjchem-1434	80	15	of	of	ADP
eurjchem-1434	80	16	the	the	DET
eurjchem-1434	80	17	studied	study	VERB
eurjchem-1434	80	18	drug	drug	NOUN
eurjchem-1434	80	19	on	on	ADP
eurjchem-1434	80	20	the	the	DET
eurjchem-1434	80	21	same	same	ADJ
eurjchem-1434	80	22	day	day	NOUN
eurjchem-1434	80	23	,	,	PUNCT
eurjchem-1434	80	24	while	while	SCONJ
eurjchem-1434	80	25	the	the	DET
eurjchem-1434	80	26	inter‐day	inter‐day	PROPN
eurjchem-1434	80	27	precision	precision	NOUN
eurjchem-1434	80	28	was	be	AUX
eurjchem-1434	80	29	evaluated	evaluate	VERB
eurjchem-1434	80	30	through	through	AUX
eurjchem-1434	80	31	replicate	replicate	VERB
eurjchem-1434	80	32	the	the	DET
eurjchem-1434	80	33	assay	assay	NOUN
eurjchem-1434	80	34	on	on	ADP
eurjchem-1434	80	35	three	three	NUM
eurjchem-1434	80	36	successive	successive	ADJ
eurjchem-1434	80	37	days	day	NOUN
eurjchem-1434	80	38	(	(	PUNCT
eurjchem-1434	80	39	table	table	NOUN
eurjchem-1434	80	40	2	2	NUM
eurjchem-1434	80	41	)	)	PUNCT
eurjchem-1434	80	42	.	.	PUNCT
eurjchem-1434	81	1	the	the	DET
eurjchem-1434	81	2	values	value	NOUN
eurjchem-1434	81	3	of	of	ADP
eurjchem-1434	81	4	standard	standard	ADJ
eurjchem-1434	81	5	deviation	deviation	NOUN
eurjchem-1434	81	6	(	(	PUNCT
eurjchem-1434	81	7	sd	sd	NOUN
eurjchem-1434	81	8	)	)	PUNCT
eurjchem-1434	81	9	were	be	AUX
eurjchem-1434	81	10	small	small	ADJ
eurjchem-1434	81	11	what	what	PRON
eurjchem-1434	81	12	indicates	indicate	VERB
eurjchem-1434	81	13	that	that	SCONJ
eurjchem-1434	81	14	the	the	DET
eurjchem-1434	81	15	repeatability	repeatability	NOUN
eurjchem-1434	81	16	of	of	ADP
eurjchem-1434	81	17	the	the	DET
eurjchem-1434	81	18	proposed	propose	VERB
eurjchem-1434	81	19	method	method	NOUN
eurjchem-1434	81	20	is	be	AUX
eurjchem-1434	81	21	good	good	ADJ
eurjchem-1434	81	22	and	and	CCONJ
eurjchem-1434	81	23	the	the	DET
eurjchem-1434	81	24	suitability	suitability	NOUN
eurjchem-1434	81	25	of	of	ADP
eurjchem-1434	81	26	the	the	DET
eurjchem-1434	81	27	lc‐ms	lc‐ms	NOUN
eurjchem-1434	81	28	/	/	SYM
eurjchem-1434	81	29	ms	ms	PROPN
eurjchem-1434	81	30	method	method	NOUN
eurjchem-1434	81	31	,	,	PUNCT
eurjchem-1434	81	32	for	for	ADP
eurjchem-1434	81	33	the	the	DET
eurjchem-1434	81	34	routine	routine	ADJ
eurjchem-1434	81	35	detection	detection	NOUN
eurjchem-1434	81	36	of	of	ADP
eurjchem-1434	81	37	acm	acm	NOUN
eurjchem-1434	81	38	in	in	ADP
eurjchem-1434	81	39	presence	presence	NOUN
eurjchem-1434	81	40	of	of	ADP
eurjchem-1434	81	41	its	its	PRON
eurjchem-1434	81	42	metabolite	metabolite	NOUN
eurjchem-1434	81	43	and	and	CCONJ
eurjchem-1434	81	44	degradations	degradation	NOUN
eurjchem-1434	81	45	products	product	NOUN
eurjchem-1434	81	46	.	.	PUNCT
eurjchem-1434	82	1	216	216	NUM
eurjchem-1434	82	2	abou‐el	abou‐el	PROPN
eurjchem-1434	82	3	alamin	alamin	PROPN
eurjchem-1434	82	4	/	/	SYM
eurjchem-1434	82	5	european	european	PROPN
eurjchem-1434	82	6	journal	journal	PROPN
eurjchem-1434	82	7	of	of	ADP
eurjchem-1434	82	8	chemistry	chemistry	NOUN
eurjchem-1434	82	9	7	7	NUM
eurjchem-1434	82	10	(	(	PUNCT
eurjchem-1434	82	11	2	2	NUM
eurjchem-1434	82	12	)	)	PUNCT
eurjchem-1434	82	13	(	(	PUNCT
eurjchem-1434	82	14	2016	2016	NUM
eurjchem-1434	82	15	)	)	PUNCT
eurjchem-1434	82	16	213‐216	213‐216	NUM
eurjchem-1434	82	17	table	table	NOUN
eurjchem-1434	82	18	1	1	NUM
eurjchem-1434	82	19	.	.	PUNCT
eurjchem-1434	82	20	validation	validation	NOUN
eurjchem-1434	82	21	parameters	parameter	NOUN
eurjchem-1434	82	22	for	for	ADP
eurjchem-1434	82	23	the	the	DET
eurjchem-1434	82	24	determination	determination	NOUN
eurjchem-1434	82	25	of	of	ADP
eurjchem-1434	82	26	pure	pure	ADJ
eurjchem-1434	82	27	acm	acm	NOUN
eurjchem-1434	82	28	by	by	ADP
eurjchem-1434	82	29	the	the	DET
eurjchem-1434	82	30	proposed	propose	VERB
eurjchem-1434	82	31	uplc‐ms	uplc‐ms	NOUN
eurjchem-1434	82	32	/	/	SYM
eurjchem-1434	82	33	ms	ms	NOUN
eurjchem-1434	82	34	method	method	NOUN
eurjchem-1434	82	35	.	.	PUNCT
eurjchem-1434	83	1	parameter	parameter	PROPN
eurjchem-1434	83	2	acm	acm	PROPN
eurjchem-1434	83	3	range	range	PROPN
eurjchem-1434	83	4	(	(	PUNCT
eurjchem-1434	83	5	ng	ng	PROPN
eurjchem-1434	83	6	/	/	SYM
eurjchem-1434	83	7	ml	ml	NOUN
eurjchem-1434	83	8	)	)	PUNCT
eurjchem-1434	83	9	8.0‐500.0	8.0‐500.0	NUM
eurjchem-1434	83	10	slope	slope	NOUN
eurjchem-1434	83	11	0.6353	0.6353	NUM
eurjchem-1434	83	12	intercept	intercept	NOUN
eurjchem-1434	83	13	‐1.044	‐1.044	ADP
eurjchem-1434	83	14	correlation	correlation	NOUN
eurjchem-1434	83	15	coefficient	coefficient	NOUN
eurjchem-1434	83	16	(	(	PUNCT
eurjchem-1434	83	17	r	r	NOUN
eurjchem-1434	83	18	)	)	PUNCT
eurjchem-1434	83	19	0.9994	0.9994	NUM
eurjchem-1434	83	20	lod	lod	PROPN
eurjchem-1434	83	21	(	(	PUNCT
eurjchem-1434	83	22	ng	ng	PROPN
eurjchem-1434	83	23	/	/	SYM
eurjchem-1434	83	24	ml	ml	NOUN
eurjchem-1434	83	25	)	)	PUNCT
eurjchem-1434	83	26	2.52	2.52	NUM
eurjchem-1434	83	27	loq	loq	PROPN
eurjchem-1434	83	28	(	(	PUNCT
eurjchem-1434	83	29	ng	ng	PROPN
eurjchem-1434	83	30	/	/	SYM
eurjchem-1434	83	31	ml	ml	NOUN
eurjchem-1434	83	32	)	)	PUNCT
eurjchem-1434	83	33	7.64	7.64	NUM
eurjchem-1434	83	34	table	table	NOUN
eurjchem-1434	83	35	2	2	NUM
eurjchem-1434	83	36	.	.	X
eurjchem-1434	83	37	accuracy	accuracy	NOUN
eurjchem-1434	83	38	and	and	CCONJ
eurjchem-1434	83	39	precision	precision	NOUN
eurjchem-1434	83	40	of	of	ADP
eurjchem-1434	83	41	the	the	DET
eurjchem-1434	83	42	proposed	propose	VERB
eurjchem-1434	83	43	uplc‐ms	uplc‐ms	NOUN
eurjchem-1434	83	44	/	/	SYM
eurjchem-1434	83	45	ms	ms	NOUN
eurjchem-1434	83	46	method	method	NOUN
eurjchem-1434	83	47	for	for	ADP
eurjchem-1434	83	48	the	the	DET
eurjchem-1434	83	49	determination	determination	NOUN
eurjchem-1434	83	50	of	of	ADP
eurjchem-1434	83	51	pure	pure	ADJ
eurjchem-1434	83	52	acm	acm	PROPN
eurjchem-1434	83	53	.	.	PUNCT
eurjchem-1434	84	1	parameter	parameter	PROPN
eurjchem-1434	84	2	proposed	propose	VERB
eurjchem-1434	84	3	uplc‐ms	uplc‐ms	PROPN
eurjchem-1434	84	4	/	/	SYM
eurjchem-1434	84	5	ms	ms	PROPN
eurjchem-1434	84	6	reported	report	VERB
eurjchem-1434	84	7	hplc	hplc	NOUN
eurjchem-1434	84	8	[	[	X
eurjchem-1434	84	9	5	5	NUM
eurjchem-1434	84	10	]	]	PUNCT
eurjchem-1434	84	11	mean±sd	mean±sd	ADP
eurjchem-1434	84	12	101.10±0.719	101.10±0.719	PROPN
eurjchem-1434	84	13	100.62±0.818	100.62±0.818	NOUN
eurjchem-1434	84	14	variance	variance	NOUN
eurjchem-1434	84	15	0.517	0.517	NUM
eurjchem-1434	84	16	0.669	0.669	NUM
eurjchem-1434	84	17	n	n	PROPN
eurjchem-1434	84	18	6	6	NUM
eurjchem-1434	84	19	6	6	NUM
eurjchem-1434	84	20	student´s	student´s	NOUN
eurjchem-1434	84	21	t‐test	t‐test	PUNCT
eurjchem-1434	84	22	(	(	PUNCT
eurjchem-1434	84	23	2.228	2.228	NUM
eurjchem-1434	84	24	)	)	PUNCT
eurjchem-1434	84	25	*	*	PUNCT
eurjchem-1434	84	26	0.790	0.790	NUM
eurjchem-1434	84	27	f‐test	f‐test	PUNCT
eurjchem-1434	84	28	(	(	PUNCT
eurjchem-1434	84	29	5.050	5.050	NUM
eurjchem-1434	84	30	)	)	PUNCT
eurjchem-1434	84	31	*	*	PUNCT
eurjchem-1434	85	1	1.294	1.294	NUM
eurjchem-1434	85	2	intra‐day	intra‐day	NOUN
eurjchem-1434	85	3	precision	precision	NOUN
eurjchem-1434	85	4	100.64±1.430	100.64±1.430	NUM
eurjchem-1434	85	5	inter‐day	inter‐day	PROPN
eurjchem-1434	85	6	precision	precision	NOUN
eurjchem-1434	85	7	101.29±1.931	101.29±1.931	NUM
eurjchem-1434	85	8	*	*	PUNCT
eurjchem-1434	85	9	the	the	DET
eurjchem-1434	85	10	values	value	NOUN
eurjchem-1434	85	11	in	in	ADP
eurjchem-1434	85	12	the	the	DET
eurjchem-1434	85	13	parentheses	parenthesis	NOUN
eurjchem-1434	85	14	are	be	AUX
eurjchem-1434	85	15	the	the	DET
eurjchem-1434	85	16	corresponding	corresponding	ADJ
eurjchem-1434	85	17	tabulated	tabulate	VERB
eurjchem-1434	85	18	values	value	NOUN
eurjchem-1434	85	19	at	at	ADP
eurjchem-1434	85	20	p	p	NOUN
eurjchem-1434	85	21	=	=	NOUN
eurjchem-1434	85	22	0.05	0.05	NUM
eurjchem-1434	85	23	.	.	PUNCT
eurjchem-1434	85	24	table	table	NOUN
eurjchem-1434	85	25	3	3	NUM
eurjchem-1434	85	26	.	.	PUNCT
eurjchem-1434	85	27	application	application	NOUN
eurjchem-1434	85	28	of	of	ADP
eurjchem-1434	85	29	the	the	DET
eurjchem-1434	85	30	proposed	propose	VERB
eurjchem-1434	85	31	method	method	NOUN
eurjchem-1434	85	32	for	for	ADP
eurjchem-1434	85	33	the	the	DET
eurjchem-1434	85	34	determination	determination	NOUN
eurjchem-1434	85	35	of	of	ADP
eurjchem-1434	85	36	acm	acm	NOUN
eurjchem-1434	85	37	in	in	ADP
eurjchem-1434	85	38	ost‐map	ost‐map	NUM
eurjchem-1434	85	39	capsules	capsule	NOUN
eurjchem-1434	85	40	.	.	PUNCT
eurjchem-1434	86	1	parameter	parameter	PROPN
eurjchem-1434	86	2	proposed	propose	VERB
eurjchem-1434	86	3	uplc‐ms	uplc‐ms	PROPN
eurjchem-1434	86	4	/	/	SYM
eurjchem-1434	86	5	ms	ms	PROPN
eurjchem-1434	86	6	reported	report	VERB
eurjchem-1434	86	7	hplc	hplc	NOUN
eurjchem-1434	87	1	[	[	X
eurjchem-1434	87	2	5	5	NUM
eurjchem-1434	87	3	]	]	PUNCT
eurjchem-1434	87	4	mean±sd	mean±sd	ADP
eurjchem-1434	87	5	99.669±3.068	99.669±3.068	NUM
eurjchem-1434	87	6	98.031±1.978	98.031±1.978	NUM
eurjchem-1434	87	7	variance	variance	NOUN
eurjchem-1434	87	8	9.413	9.413	NUM
eurjchem-1434	87	9	3.912	3.912	NUM
eurjchem-1434	87	10	n	n	NUM
eurjchem-1434	87	11	6	6	NUM
eurjchem-1434	87	12	6	6	NUM
eurjchem-1434	87	13	student´s	student´s	NOUN
eurjchem-1434	87	14	t‐test	t‐test	PUNCT
eurjchem-1434	87	15	(	(	PUNCT
eurjchem-1434	87	16	2.228	2.228	NUM
eurjchem-1434	87	17	)	)	PUNCT
eurjchem-1434	87	18	*	*	PUNCT
eurjchem-1434	87	19	0.769	0.769	NUM
eurjchem-1434	87	20	f‐test	f‐test	SYM
eurjchem-1434	87	21	(	(	PUNCT
eurjchem-1434	87	22	5.050	5.050	NUM
eurjchem-1434	87	23	)	)	PUNCT
eurjchem-1434	87	24	*	*	PUNCT
eurjchem-1434	88	1	2.406	2.406	NUM
eurjchem-1434	88	2	*	*	PUNCT
eurjchem-1434	88	3	the	the	DET
eurjchem-1434	88	4	values	value	NOUN
eurjchem-1434	88	5	in	in	ADP
eurjchem-1434	88	6	the	the	DET
eurjchem-1434	88	7	parentheses	parenthesis	NOUN
eurjchem-1434	88	8	are	be	AUX
eurjchem-1434	88	9	the	the	DET
eurjchem-1434	88	10	corresponding	corresponding	ADJ
eurjchem-1434	88	11	tabulated	tabulate	VERB
eurjchem-1434	88	12	values	value	NOUN
eurjchem-1434	88	13	at	at	ADP
eurjchem-1434	88	14	p	p	NOUN
eurjchem-1434	88	15	=	=	PROPN
eurjchem-1434	88	16	0.05	0.05	NUM
eurjchem-1434	88	17	.	.	PUNCT
eurjchem-1434	89	1	3.3.4	3.3.4	NUM
eurjchem-1434	89	2	.	.	PUNCT
eurjchem-1434	90	1	robustness	robustness	NOUN
eurjchem-1434	90	2	of	of	ADP
eurjchem-1434	90	3	the	the	DET
eurjchem-1434	90	4	method	method	NOUN
eurjchem-1434	90	5	the	the	DET
eurjchem-1434	90	6	robustness	robustness	NOUN
eurjchem-1434	90	7	of	of	ADP
eurjchem-1434	90	8	analytical	analytical	ADJ
eurjchem-1434	90	9	method	method	NOUN
eurjchem-1434	90	10	measures	measure	VERB
eurjchem-1434	90	11	the	the	DET
eurjchem-1434	90	12	capacity	capacity	NOUN
eurjchem-1434	90	13	of	of	ADP
eurjchem-1434	90	14	it	it	PRON
eurjchem-1434	90	15	to	to	PART
eurjchem-1434	90	16	restrain	restrain	VERB
eurjchem-1434	90	17	small	small	ADJ
eurjchem-1434	90	18	but	but	CCONJ
eurjchem-1434	90	19	deliberate	deliberate	ADJ
eurjchem-1434	90	20	changes	change	NOUN
eurjchem-1434	90	21	in	in	ADP
eurjchem-1434	90	22	method	method	NOUN
eurjchem-1434	90	23	parameters	parameter	NOUN
eurjchem-1434	90	24	.	.	PUNCT
eurjchem-1434	91	1	evaluation	evaluation	NOUN
eurjchem-1434	91	2	of	of	ADP
eurjchem-1434	91	3	the	the	DET
eurjchem-1434	91	4	robustness	robustness	NOUN
eurjchem-1434	91	5	of	of	ADP
eurjchem-1434	91	6	the	the	DET
eurjchem-1434	91	7	proposed	propose	VERB
eurjchem-1434	91	8	method	method	NOUN
eurjchem-1434	91	9	was	be	AUX
eurjchem-1434	91	10	done	do	VERB
eurjchem-1434	91	11	for	for	ADP
eurjchem-1434	91	12	the	the	DET
eurjchem-1434	91	13	chromatographic	chromatographic	ADJ
eurjchem-1434	91	14	parameters	parameter	NOUN
eurjchem-1434	91	15	as	as	ADV
eurjchem-1434	91	16	well	well	ADV
eurjchem-1434	91	17	as	as	ADP
eurjchem-1434	91	18	,	,	PUNCT
eurjchem-1434	91	19	the	the	DET
eurjchem-1434	91	20	mass	mass	NOUN
eurjchem-1434	91	21	parameters	parameter	NOUN
eurjchem-1434	91	22	,	,	PUNCT
eurjchem-1434	91	23	e.g.	e.g.	ADV
eurjchem-1434	91	24	flow	flow	NOUN
eurjchem-1434	91	25	rate	rate	NOUN
eurjchem-1434	91	26	of	of	ADP
eurjchem-1434	91	27	mobile	mobile	ADJ
eurjchem-1434	91	28	phase	phase	NOUN
eurjchem-1434	91	29	(	(	PUNCT
eurjchem-1434	91	30	±10	±10	NOUN
eurjchem-1434	91	31	μl	μl	ADP
eurjchem-1434	91	32	/	/	SYM
eurjchem-1434	91	33	min	min	NOUN
eurjchem-1434	91	34	)	)	PUNCT
eurjchem-1434	91	35	,	,	PUNCT
eurjchem-1434	91	36	vaporizer	vaporizer	NOUN
eurjchem-1434	91	37	temperature	temperature	NOUN
eurjchem-1434	91	38	or	or	CCONJ
eurjchem-1434	91	39	transfer	transfer	VERB
eurjchem-1434	91	40	capillary	capillary	ADJ
eurjchem-1434	91	41	temperature	temperature	NOUN
eurjchem-1434	91	42	(	(	PUNCT
eurjchem-1434	91	43	±5	±5	VERB
eurjchem-1434	92	1	°	°	NOUN
eurjchem-1434	92	2	c	c	NOUN
eurjchem-1434	92	3	)	)	PUNCT
eurjchem-1434	93	1	,	,	PUNCT
eurjchem-1434	93	2	collision	collision	VERB
eurjchem-1434	93	3	energy	energy	NOUN
eurjchem-1434	93	4	(	(	PUNCT
eurjchem-1434	93	5	±2	±2	NOUN
eurjchem-1434	93	6	v	v	NOUN
eurjchem-1434	93	7	)	)	PUNCT
eurjchem-1434	93	8	and	and	CCONJ
eurjchem-1434	93	9	sheath	sheath	NOUN
eurjchem-1434	93	10	gas	gas	NOUN
eurjchem-1434	93	11	pressure	pressure	NOUN
eurjchem-1434	93	12	(	(	PUNCT
eurjchem-1434	93	13	±5	±5	NOUN
eurjchem-1434	93	14	psi	psi	NOUN
eurjchem-1434	93	15	)	)	PUNCT
eurjchem-1434	93	16	did	do	AUX
eurjchem-1434	93	17	not	not	PART
eurjchem-1434	93	18	show	show	VERB
eurjchem-1434	93	19	significant	significant	ADJ
eurjchem-1434	93	20	changes	change	NOUN
eurjchem-1434	93	21	in	in	ADP
eurjchem-1434	93	22	the	the	DET
eurjchem-1434	93	23	values	value	NOUN
eurjchem-1434	93	24	of	of	ADP
eurjchem-1434	93	25	peak	peak	NOUN
eurjchem-1434	93	26	areas	area	NOUN
eurjchem-1434	93	27	of	of	ADP
eurjchem-1434	93	28	acm	acm	PROPN
eurjchem-1434	93	29	.	.	PUNCT
eurjchem-1434	94	1	3.4	3.4	NUM
eurjchem-1434	94	2	.	.	PUNCT
eurjchem-1434	94	3	application	application	NOUN
eurjchem-1434	94	4	of	of	ADP
eurjchem-1434	94	5	the	the	DET
eurjchem-1434	94	6	proposed	propose	VERB
eurjchem-1434	94	7	method	method	NOUN
eurjchem-1434	94	8	the	the	DET
eurjchem-1434	94	9	proposed	propose	VERB
eurjchem-1434	94	10	uplc‐ms	uplc‐ms	NOUN
eurjchem-1434	94	11	/	/	SYM
eurjchem-1434	94	12	ms	ms	NOUN
eurjchem-1434	94	13	method	method	NOUN
eurjchem-1434	94	14	was	be	AUX
eurjchem-1434	94	15	successfully	successfully	ADV
eurjchem-1434	94	16	applied	apply	VERB
eurjchem-1434	94	17	for	for	ADP
eurjchem-1434	94	18	the	the	DET
eurjchem-1434	94	19	determination	determination	NOUN
eurjchem-1434	94	20	of	of	ADP
eurjchem-1434	94	21	acm	acm	NOUN
eurjchem-1434	94	22	in	in	ADP
eurjchem-1434	94	23	its	its	PRON
eurjchem-1434	94	24	dosage	dosage	NOUN
eurjchem-1434	94	25	form	form	NOUN
eurjchem-1434	94	26	with	with	ADP
eurjchem-1434	94	27	satisfactory	satisfactory	ADJ
eurjchem-1434	94	28	recovery	recovery	NOUN
eurjchem-1434	94	29	.	.	PUNCT
eurjchem-1434	95	1	the	the	DET
eurjchem-1434	95	2	obtained	obtain	VERB
eurjchem-1434	95	3	results	result	NOUN
eurjchem-1434	95	4	are	be	AUX
eurjchem-1434	95	5	listed	list	VERB
eurjchem-1434	95	6	in	in	ADP
eurjchem-1434	95	7	table	table	NOUN
eurjchem-1434	95	8	3	3	NUM
eurjchem-1434	95	9	.	.	NOUN
eurjchem-1434	95	10	4	4	NUM
eurjchem-1434	95	11	.	.	X
eurjchem-1434	95	12	conclusion	conclusion	NOUN
eurjchem-1434	95	13	specific	specific	ADJ
eurjchem-1434	95	14	and	and	CCONJ
eurjchem-1434	95	15	sensitive	sensitive	ADJ
eurjchem-1434	95	16	ultra‐performance	ultra‐performance	ADP
eurjchem-1434	95	17	liquid	liquid	NOUN
eurjchem-1434	95	18	chroma‐	chroma‐	NUM
eurjchem-1434	95	19	tography	tography	NOUN
eurjchem-1434	95	20	coupled	couple	VERB
eurjchem-1434	95	21	to	to	PART
eurjchem-1434	95	22	tandem	tandem	VERB
eurjchem-1434	95	23	mass	mass	ADJ
eurjchem-1434	95	24	spectrometric	spectrometric	ADJ
eurjchem-1434	95	25	technique	technique	NOUN
eurjchem-1434	95	26	(	(	PUNCT
eurjchem-1434	95	27	uplc‐ms	uplc‐ms	NOUN
eurjchem-1434	95	28	/	/	SYM
eurjchem-1434	95	29	ms	ms	NOUN
eurjchem-1434	95	30	)	)	PUNCT
eurjchem-1434	95	31	was	be	AUX
eurjchem-1434	95	32	developed	develop	VERB
eurjchem-1434	95	33	for	for	ADP
eurjchem-1434	95	34	simultaneous	simultaneous	ADJ
eurjchem-1434	95	35	determi‐	determi‐	PRON
eurjchem-1434	95	36	nation	nation	NOUN
eurjchem-1434	95	37	of	of	ADP
eurjchem-1434	95	38	acemetacin	acemetacin	PROPN
eurjchem-1434	95	39	(	(	PUNCT
eurjchem-1434	95	40	acm	acm	PROPN
eurjchem-1434	95	41	)	)	PUNCT
eurjchem-1434	95	42	in	in	ADP
eurjchem-1434	95	43	presence	presence	NOUN
eurjchem-1434	95	44	of	of	ADP
eurjchem-1434	95	45	its	its	PRON
eurjchem-1434	95	46	metabolite	metabolite	NOUN
eurjchem-1434	95	47	(	(	PUNCT
eurjchem-1434	95	48	indomethacin	indomethacin	PROPN
eurjchem-1434	95	49	)	)	PUNCT
eurjchem-1434	95	50	and	and	CCONJ
eurjchem-1434	95	51	degradation	degradation	NOUN
eurjchem-1434	95	52	products	product	NOUN
eurjchem-1434	95	53	.	.	PUNCT
eurjchem-1434	96	1	different	different	ADJ
eurjchem-1434	96	2	chroma‐	chroma‐	NUM
eurjchem-1434	96	3	tographic	tographic	ADJ
eurjchem-1434	96	4	parameters	parameter	NOUN
eurjchem-1434	96	5	and	and	CCONJ
eurjchem-1434	96	6	mass	mass	ADJ
eurjchem-1434	96	7	spectrometric	spectrometric	ADJ
eurjchem-1434	96	8	conditions	condition	NOUN
eurjchem-1434	96	9	were	be	AUX
eurjchem-1434	96	10	investigated	investigate	VERB
eurjchem-1434	96	11	to	to	PART
eurjchem-1434	96	12	select	select	VERB
eurjchem-1434	96	13	the	the	DET
eurjchem-1434	96	14	optimum	optimum	ADJ
eurjchem-1434	96	15	conditions	condition	NOUN
eurjchem-1434	96	16	for	for	ADP
eurjchem-1434	96	17	the	the	DET
eurjchem-1434	96	18	separation	separation	NOUN
eurjchem-1434	96	19	.	.	PUNCT
eurjchem-1434	97	1	the	the	DET
eurjchem-1434	97	2	method	method	NOUN
eurjchem-1434	97	3	was	be	AUX
eurjchem-1434	97	4	validated	validate	VERB
eurjchem-1434	97	5	according	accord	VERB
eurjchem-1434	97	6	to	to	ADP
eurjchem-1434	97	7	ich	ich	NOUN
eurjchem-1434	97	8	guidelines	guideline	NOUN
eurjchem-1434	97	9	and	and	CCONJ
eurjchem-1434	97	10	successfully	successfully	ADV
eurjchem-1434	97	11	applied	apply	VERB
eurjchem-1434	97	12	for	for	ADP
eurjchem-1434	97	13	the	the	DET
eurjchem-1434	97	14	determination	determination	NOUN
eurjchem-1434	97	15	of	of	ADP
eurjchem-1434	97	16	cited	cite	VERB
eurjchem-1434	97	17	drug	drug	NOUN
eurjchem-1434	97	18	in	in	ADP
eurjchem-1434	97	19	dosage	dosage	NOUN
eurjchem-1434	97	20	form	form	NOUN
eurjchem-1434	97	21	.	.	PUNCT
eurjchem-1434	98	1	acknowledgements	acknowledgement	VERB
eurjchem-1434	98	2	the	the	DET
eurjchem-1434	98	3	author	author	NOUN
eurjchem-1434	98	4	thanks	thanks	PROPN
eurjchem-1434	98	5	department	department	PROPN
eurjchem-1434	98	6	of	of	ADP
eurjchem-1434	98	7	analytical	analytical	ADJ
eurjchem-1434	98	8	chemistry	chemistry	NOUN
eurjchem-1434	98	9	,	,	PUNCT
eurjchem-1434	98	10	faculty	faculty	NOUN
eurjchem-1434	98	11	of	of	ADP
eurjchem-1434	98	12	pharmacy	pharmacy	NOUN
eurjchem-1434	98	13	,	,	PUNCT
eurjchem-1434	98	14	helwan	helwan	PROPN
eurjchem-1434	98	15	university	university	NOUN
eurjchem-1434	98	16	for	for	ADP
eurjchem-1434	98	17	providing	provide	VERB
eurjchem-1434	98	18	instruments	instrument	NOUN
eurjchem-1434	98	19	and	and	CCONJ
eurjchem-1434	98	20	national	national	ADJ
eurjchem-1434	98	21	organization	organization	NOUN
eurjchem-1434	98	22	for	for	ADP
eurjchem-1434	98	23	drug	drug	NOUN
eurjchem-1434	98	24	control	control	NOUN
eurjchem-1434	98	25	and	and	CCONJ
eurjchem-1434	98	26	research	research	NOUN
eurjchem-1434	98	27	(	(	PUNCT
eurjchem-1434	98	28	nodcar	nodcar	NOUN
eurjchem-1434	98	29	)	)	PUNCT
eurjchem-1434	98	30	,	,	PUNCT
eurjchem-1434	98	31	cairo	cairo	PROPN
eurjchem-1434	98	32	,	,	PUNCT
eurjchem-1434	98	33	egypt	egypt	PROPN
eurjchem-1434	98	34	for	for	ADP
eurjchem-1434	98	35	supplying	supply	VERB
eurjchem-1434	98	36	the	the	DET
eurjchem-1434	98	37	standard	standard	ADJ
eurjchem-1434	98	38	materials	material	NOUN
eurjchem-1434	98	39	during	during	ADP
eurjchem-1434	98	40	this	this	DET
eurjchem-1434	98	41	work	work	NOUN
eurjchem-1434	98	42	.	.	PUNCT
eurjchem-1434	99	1	references	reference	NOUN
eurjchem-1434	99	2	[	[	X
eurjchem-1434	99	3	1	1	NUM
eurjchem-1434	99	4	]	]	PUNCT
eurjchem-1434	99	5	.	.	PUNCT
eurjchem-1434	100	1	acemetacin	acemetacin	PROPN
eurjchem-1434	100	2	,	,	PUNCT
eurjchem-1434	100	3	wikipedia	wikipedia	PROPN
eurjchem-1434	100	4	,	,	PUNCT
eurjchem-1434	100	5	the	the	DET
eurjchem-1434	100	6	free	free	ADJ
eurjchem-1434	100	7	encyclopaedia	encyclopaedia	NOUN
eurjchem-1434	100	8	,	,	PUNCT
eurjchem-1434	100	9	https://en.wikipedia.org/wiki/acemetacin	https://en.wikipedia.org/wiki/acemetacin	PROPN
eurjchem-1434	101	1	[	[	X
eurjchem-1434	101	2	2	2	NUM
eurjchem-1434	101	3	]	]	PUNCT
eurjchem-1434	101	4	.	.	PUNCT
eurjchem-1434	102	1	ozbakan	ozbakan	PROPN
eurjchem-1434	102	2	,	,	PUNCT
eurjchem-1434	102	3	h.	h.	PROPN
eurjchem-1434	102	4	;	;	PUNCT
eurjchem-1434	102	5	palabiyik	palabiyik	NOUN
eurjchem-1434	102	6	,	,	PUNCT
eurjchem-1434	102	7	i.	i.	NOUN
eurjchem-1434	102	8	m.	m.	NOUN
eurjchem-1434	102	9	;	;	PUNCT
eurjchem-1434	102	10	caglayan	caglayan	NOUN
eurjchem-1434	102	11	,	,	PUNCT
eurjchem-1434	102	12	m.	m.	NOUN
eurjchem-1434	102	13	g.	g.	PROPN
eurjchem-1434	102	14	;	;	PUNCT
eurjchem-1434	102	15	onur	onur	PROPN
eurjchem-1434	102	16	,	,	PUNCT
eurjchem-1434	102	17	f.	f.	PROPN
eurjchem-1434	102	18	turk	turk	PROPN
eurjchem-1434	102	19	.	.	PUNCT
eurjchem-1434	103	1	j.	j.	PROPN
eurjchem-1434	103	2	pharm	pharm	PROPN
eurjchem-1434	103	3	.	.	PUNCT
eurjchem-1434	104	1	sci	sci	PROPN
eurjchem-1434	104	2	.	.	PROPN
eurjchem-1434	104	3	2009	2009	NUM
eurjchem-1434	104	4	,	,	PUNCT
eurjchem-1434	104	5	6	6	NUM
eurjchem-1434	104	6	,	,	PUNCT
eurjchem-1434	104	7	163‐176	163‐176	PROPN
eurjchem-1434	104	8	.	.	PUNCT
eurjchem-1434	105	1	[	[	X
eurjchem-1434	105	2	3	3	NUM
eurjchem-1434	105	3	]	]	PUNCT
eurjchem-1434	105	4	.	.	PUNCT
eurjchem-1434	106	1	naguib	naguib	PROPN
eurjchem-1434	106	2	,	,	PUNCT
eurjchem-1434	106	3	i.	i.	PROPN
eurjchem-1434	106	4	a.	a.	PROPN
eurjchem-1434	106	5	;	;	PUNCT
eurjchem-1434	106	6	abdel‐aleem	abdel‐aleem	PROPN
eurjchem-1434	106	7	,	,	PUNCT
eurjchem-1434	106	8	e.	e.	PROPN
eurjchem-1434	106	9	a.	a.	PROPN
eurjchem-1434	106	10	;	;	PUNCT
eurjchem-1434	106	11	zaazaa	zaazaa	PROPN
eurjchem-1434	106	12	,	,	PUNCT
eurjchem-1434	106	13	h.	h.	PROPN
eurjchem-1434	106	14	;	;	PUNCT
eurjchem-1434	106	15	hussein	hussein	PROPN
eurjchem-1434	106	16	,	,	PUNCT
eurjchem-1434	106	17	e.	e.	PROPN
eurjchem-1434	106	18	a.	a.	PROPN
eurjchem-1434	106	19	eur	eur	PROPN
eurjchem-1434	106	20	.	.	PUNCT
eurjchem-1434	107	1	j.	j.	PROPN
eurjchem-1434	107	2	chem	chem	PROPN
eurjchem-1434	107	3	.	.	PUNCT
eurjchem-1434	108	1	2014	2014	NUM
eurjchem-1434	108	2	,	,	PUNCT
eurjchem-1434	108	3	5	5	NUM
eurjchem-1434	108	4	,	,	PUNCT
eurjchem-1434	108	5	219‐226	219‐226	NUM
eurjchem-1434	108	6	.	.	PUNCT
eurjchem-1434	109	1	[	[	X
eurjchem-1434	109	2	4	4	NUM
eurjchem-1434	109	3	]	]	PUNCT
eurjchem-1434	109	4	.	.	PUNCT
eurjchem-1434	109	5	walash	walash	NOUN
eurjchem-1434	109	6	,	,	PUNCT
eurjchem-1434	109	7	m.	m.	NOUN
eurjchem-1434	109	8	i.	i.	PROPN
eurjchem-1434	109	9	;	;	PUNCT
eurjchem-1434	109	10	belal	belal	PROPN
eurjchem-1434	109	11	,	,	PUNCT
eurjchem-1434	109	12	f.	f.	PROPN
eurjchem-1434	109	13	;	;	PUNCT
eurjchem-1434	109	14	tolba	tolba	PROPN
eurjchem-1434	109	15	,	,	PUNCT
eurjchem-1434	109	16	m.	m.	NOUN
eurjchem-1434	109	17	m.	m.	NOUN
eurjchem-1434	109	18	;	;	PUNCT
eurjchem-1434	109	19	halawa	halawa	PROPN
eurjchem-1434	109	20	,	,	PUNCT
eurjchem-1434	109	21	m.	m.	NOUN
eurjchem-1434	109	22	i.	i.	PROPN
eurjchem-1434	109	23	sep	sep	PROPN
eurjchem-1434	109	24	.	.	PUNCT
eurjchem-1434	110	1	sci	sci	PROPN
eurjchem-1434	110	2	.	.	PUNCT
eurjchem-1434	110	3	tech	tech	PROPN
eurjchem-1434	110	4	.	.	PUNCT
eurjchem-1434	111	1	2015	2015	NUM
eurjchem-1434	111	2	,	,	PUNCT
eurjchem-1434	111	3	50	50	NUM
eurjchem-1434	111	4	,	,	PUNCT
eurjchem-1434	111	5	1403‐1412	1403‐1412	NUM
eurjchem-1434	111	6	.	.	PUNCT
eurjchem-1434	112	1	[	[	X
eurjchem-1434	112	2	5	5	NUM
eurjchem-1434	112	3	]	]	PUNCT
eurjchem-1434	112	4	.	.	PUNCT
eurjchem-1434	113	1	kessiba	kessiba	PROPN
eurjchem-1434	113	2	,	,	PUNCT
eurjchem-1434	113	3	a.	a.	NOUN
eurjchem-1434	113	4	m.	m.	NOUN
eurjchem-1434	113	5	;	;	PUNCT
eurjchem-1434	113	6	hegazy	hegazy	ADV
eurjchem-1434	113	7	,	,	PUNCT
eurjchem-1434	113	8	m.	m.	NOUN
eurjchem-1434	113	9	a.	a.	NOUN
eurjchem-1434	113	10	m.	m.	PROPN
eurjchem-1434	113	11	;	;	PUNCT
eurjchem-1434	113	12	abdelkawy	abdelkawy	PROPN
eurjchem-1434	113	13	,	,	PUNCT
eurjchem-1434	113	14	m.	m.	NOUN
eurjchem-1434	113	15	m.	m.	NOUN
eurjchem-1434	113	16	;	;	PUNCT
eurjchem-1434	113	17	el	el	PROPN
eurjchem-1434	113	18	gendy	gendy	PROPN
eurjchem-1434	113	19	,	,	PUNCT
eurjchem-1434	113	20	a.	a.	PROPN
eurjchem-1434	113	21	e.	e.	PROPN
eurjchem-1434	113	22	eur	eur	PROPN
eurjchem-1434	113	23	.	.	PUNCT
eurjchem-1434	114	1	j.	j.	PROPN
eurjchem-1434	114	2	chem	chem	PROPN
eurjchem-1434	114	3	.	.	PUNCT
eurjchem-1434	115	1	2015	2015	NUM
eurjchem-1434	115	2	,	,	PUNCT
eurjchem-1434	115	3	6(4	6(4	NUM
eurjchem-1434	115	4	)	)	PUNCT
eurjchem-1434	115	5	,	,	PUNCT
eurjchem-1434	115	6	422‐429	422‐429	NOUN
eurjchem-1434	115	7	.	.	PUNCT
eurjchem-1434	116	1	[	[	X
eurjchem-1434	116	2	6	6	NUM
eurjchem-1434	116	3	]	]	PUNCT
eurjchem-1434	116	4	.	.	PUNCT
eurjchem-1434	117	1	ban	ban	PROPN
eurjchem-1434	117	2	,	,	PUNCT
eurjchem-1434	117	3	e.	e.	PROPN
eurjchem-1434	117	4	;	;	PUNCT
eurjchem-1434	117	5	cho	cho	PROPN
eurjchem-1434	117	6	,	,	PUNCT
eurjchem-1434	117	7	j.	j.	PROPN
eurjchem-1434	117	8	h.	h.	PROPN
eurjchem-1434	117	9	;	;	PUNCT
eurjchem-1434	117	10	jang	jang	PROPN
eurjchem-1434	117	11	,	,	PUNCT
eurjchem-1434	117	12	d.	d.	PROPN
eurjchem-1434	117	13	j.	j.	PROPN
eurjchem-1434	117	14	;	;	PUNCT
eurjchem-1434	117	15	piao	piao	PROPN
eurjchem-1434	117	16	,	,	PUNCT
eurjchem-1434	117	17	x.	x.	PROPN
eurjchem-1434	117	18	l.	l.	PROPN
eurjchem-1434	117	19	;	;	PUNCT
eurjchem-1434	117	20	kim	kim	PROPN
eurjchem-1434	117	21	,	,	PUNCT
eurjchem-1434	117	22	c.	c.	PROPN
eurjchem-1434	117	23	k.	k.	PROPN
eurjchem-1434	117	24	j.	j.	PROPN
eurjchem-1434	117	25	liq	liq	PROPN
eurjchem-1434	117	26	.	.	PUNCT
eurjchem-1434	118	1	chrom	chrom	PROPN
eurjchem-1434	118	2	.	.	PUNCT
eurjchem-1434	119	1	rel	rel	PROPN
eurjchem-1434	119	2	.	.	PUNCT
eurjchem-1434	120	1	tech	tech	NOUN
eurjchem-1434	120	2	.	.	PUNCT
eurjchem-1434	121	1	2005	2005	NUM
eurjchem-1434	121	2	,	,	PUNCT
eurjchem-1434	121	3	28	28	NUM
eurjchem-1434	121	4	,	,	PUNCT
eurjchem-1434	121	5	1593‐1604	1593‐1604	NUM
eurjchem-1434	121	6	.	.	PUNCT
eurjchem-1434	122	1	[	[	X
eurjchem-1434	122	2	7	7	NUM
eurjchem-1434	122	3	]	]	PUNCT
eurjchem-1434	122	4	.	.	PUNCT
eurjchem-1434	123	1	reguera	reguera	NOUN
eurjchem-1434	123	2	,	,	PUNCT
eurjchem-1434	123	3	c.	c.	PROPN
eurjchem-1434	123	4	;	;	PUNCT
eurjchem-1434	123	5	arcos	arcos	PROPN
eurjchem-1434	123	6	,	,	PUNCT
eurjchem-1434	123	7	m.	m.	NOUN
eurjchem-1434	123	8	j.	j.	PROPN
eurjchem-1434	123	9	;	;	PUNCT
eurjchem-1434	123	10	ortiz	ortiz	PROPN
eurjchem-1434	123	11	,	,	PUNCT
eurjchem-1434	123	12	m.	m.	PROPN
eurjchem-1434	123	13	c.	c.	PROPN
eurjchem-1434	123	14	talanta	talanta	PROPN
eurjchem-1434	123	15	1998	1998	NUM
eurjchem-1434	123	16	,	,	PUNCT
eurjchem-1434	123	17	46	46	NUM
eurjchem-1434	123	18	,	,	PUNCT
eurjchem-1434	123	19	1493‐1505	1493‐1505	NUM
eurjchem-1434	123	20	.	.	PUNCT
eurjchem-1434	124	1	[	[	X
eurjchem-1434	124	2	8	8	NUM
eurjchem-1434	124	3	]	]	PUNCT
eurjchem-1434	124	4	.	.	PUNCT
eurjchem-1434	125	1	reguera	reguera	NOUN
eurjchem-1434	125	2	,	,	PUNCT
eurjchem-1434	125	3	c.	c.	PROPN
eurjchem-1434	125	4	;	;	PUNCT
eurjchem-1434	125	5	ortiz	ortiz	PROPN
eurjchem-1434	125	6	,	,	PUNCT
eurjchem-1434	125	7	m.	m.	PROPN
eurjchem-1434	125	8	c.	c.	PROPN
eurjchem-1434	125	9	;	;	PUNCT
eurjchem-1434	125	10	arcos	arcos	PROPN
eurjchem-1434	125	11	,	,	PUNCT
eurjchem-1434	125	12	m.	m.	NOUN
eurjchem-1434	125	13	j.	j.	PROPN
eurjchem-1434	125	14	electroanal	electroanal	PROPN
eurjchem-1434	125	15	.	.	PUNCT
eurjchem-1434	126	1	2002	2002	NUM
eurjchem-1434	126	2	,	,	PUNCT
eurjchem-1434	126	3	14	14	NUM
eurjchem-1434	126	4	,	,	PUNCT
eurjchem-1434	126	5	1699‐1706	1699‐1706	NUM
eurjchem-1434	126	6	.	.	PUNCT
eurjchem-1434	127	1	[	[	X
eurjchem-1434	127	2	9	9	NUM
eurjchem-1434	127	3	]	]	PUNCT
eurjchem-1434	127	4	.	.	PUNCT
eurjchem-1434	128	1	british	british	PROPN
eurjchem-1434	128	2	pharmacopoeia	pharmacopoeia	PROPN
eurjchem-1434	128	3	;	;	PUNCT
eurjchem-1434	128	4	british	british	ADJ
eurjchem-1434	128	5	pharmacopoeia	pharmacopoeia	PROPN
eurjchem-1434	128	6	commission	commission	PROPN
eurjchem-1434	128	7	;	;	PUNCT
eurjchem-1434	128	8	the	the	DET
eurjchem-1434	128	9	stationary	stationary	ADJ
eurjchem-1434	128	10	office	office	NOUN
eurjchem-1434	128	11	,	,	PUNCT
eurjchem-1434	128	12	2012	2012	NUM
eurjchem-1434	128	13	.	.	PUNCT
eurjchem-1434	129	1	[	[	X
eurjchem-1434	129	2	10	10	NUM
eurjchem-1434	129	3	]	]	PUNCT
eurjchem-1434	129	4	.	.	PUNCT
eurjchem-1434	130	1	mowaka	mowaka	PROPN
eurjchem-1434	130	2	,	,	PUNCT
eurjchem-1434	130	3	s.	s.	PROPN
eurjchem-1434	130	4	;	;	PUNCT
eurjchem-1434	130	5	mohamed	mohamed	PROPN
eurjchem-1434	130	6	,	,	PUNCT
eurjchem-1434	130	7	d.	d.	PROPN
eurjchem-1434	130	8	rsc	rsc	PROPN
eurjchem-1434	130	9	adv	adv	PROPN
eurjchem-1434	130	10	.	.	PROPN
eurjchem-1434	130	11	2015	2015	NUM
eurjchem-1434	130	12	,	,	PUNCT
eurjchem-1434	130	13	5	5	NUM
eurjchem-1434	130	14	,	,	PUNCT
eurjchem-1434	130	15	60467‐60481	60467‐60481	NUM
eurjchem-1434	130	16	.	.	PUNCT
eurjchem-1434	131	1	[	[	X
eurjchem-1434	131	2	11	11	NUM
eurjchem-1434	131	3	]	]	PUNCT
eurjchem-1434	131	4	.	.	PUNCT
eurjchem-1434	131	5	ich	ich	PROPN
eurjchem-1434	131	6	,	,	PUNCT
eurjchem-1434	131	7	harmonized	harmonized	ADJ
eurjchem-1434	131	8	tripartite	tripartite	ADJ
eurjchem-1434	131	9	guideline	guideline	NOUN
eurjchem-1434	131	10	,	,	PUNCT
eurjchem-1434	131	11	validation	validation	NOUN
eurjchem-1434	131	12	of	of	ADP
eurjchem-1434	131	13	analytical	analytical	ADJ
eurjchem-1434	131	14	procedures	procedure	NOUN
eurjchem-1434	131	15	:	:	PUNCT
eurjchem-1434	131	16	text	text	NOUN
eurjchem-1434	131	17	and	and	CCONJ
eurjchem-1434	131	18	methodology	methodology	NOUN
eurjchem-1434	131	19	,	,	PUNCT
eurjchem-1434	131	20	q2(r1	q2(r1	PROPN
eurjchem-1434	131	21	)	)	PUNCT
eurjchem-1434	131	22	,	,	PUNCT
eurjchem-1434	131	23	parent	parent	NOUN
eurjchem-1434	131	24	guidelines	guideline	NOUN
eurjchem-1434	131	25	on	on	ADP
eurjchem-1434	131	26	methodology	methodology	NOUN
eurjchem-1434	131	27	,	,	PUNCT
eurjchem-1434	131	28	2005	2005	NUM
eurjchem-1434	131	29	.	.	PUNCT