id	sid	tid	token	lemma	pos
eurjchem-1477	1	1	untitled	untitle	VERB
eurjchem-1477	1	2	european	european	PROPN
eurjchem-1477	1	3	journal	journal	PROPN
eurjchem-1477	1	4	of	of	ADP
eurjchem-1477	1	5	chemistry	chemistry	NOUN
eurjchem-1477	1	6	7	7	NUM
eurjchem-1477	1	7	(	(	PUNCT
eurjchem-1477	1	8	4	4	NUM
eurjchem-1477	1	9	)	)	PUNCT
eurjchem-1477	1	10	(	(	PUNCT
eurjchem-1477	1	11	2016	2016	NUM
eurjchem-1477	1	12	)	)	PUNCT
eurjchem-1477	1	13	391‐396	391‐396	NUM
eurjchem-1477	1	14	european	european	PROPN
eurjchem-1477	1	15	journal	journal	PROPN
eurjchem-1477	1	16	of	of	ADP
eurjchem-1477	1	17	chemistry	chemistry	NOUN
eurjchem-1477	1	18	issn	issn	PROPN
eurjchem-1477	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-1477	1	20	(	(	PUNCT
eurjchem-1477	1	21	print	print	NOUN
eurjchem-1477	1	22	)	)	PUNCT
eurjchem-1477	1	23	/	/	SYM
eurjchem-1477	1	24	issn	issn	PROPN
eurjchem-1477	1	25	2153‐2257	2153‐2257	NUM
eurjchem-1477	1	26	(	(	PUNCT
eurjchem-1477	1	27	online	online	ADJ
eurjchem-1477	1	28	)	)	PUNCT
eurjchem-1477	1	29			NOUN
eurjchem-1477	1	30	2016	2016	NUM
eurjchem-1477	1	31	atlanta	atlanta	PROPN
eurjchem-1477	1	32	publishing	publishing	PROPN
eurjchem-1477	1	33	house	house	PROPN
eurjchem-1477	1	34	llc	llc	PROPN
eurjchem-1477	1	35	‐	‐	PUNCT
eurjchem-1477	1	36	all	all	DET
eurjchem-1477	1	37	rights	right	NOUN
eurjchem-1477	1	38	reserved	reserve	VERB
eurjchem-1477	1	39	‐	‐	NOUN
eurjchem-1477	1	40	printed	print	VERB
eurjchem-1477	1	41	in	in	ADP
eurjchem-1477	1	42	the	the	DET
eurjchem-1477	1	43	usa	usa	PROPN
eurjchem-1477	1	44	http://dx.doi.org/10.5155/eurjchem.7.4.391-396.1477	http://dx.doi.org/10.5155/eurjchem.7.4.391-396.1477	PROPN
eurjchem-1477	1	45	european	european	PROPN
eurjchem-1477	1	46	journal	journal	PROPN
eurjchem-1477	1	47	of	of	ADP
eurjchem-1477	1	48	chemistry	chemistry	PROPN
eurjchem-1477	1	49	journal	journal	PROPN
eurjchem-1477	1	50	webpage	webpage	NOUN
eurjchem-1477	1	51	:	:	PUNCT
eurjchem-1477	1	52	www.eurjchem.com	www.eurjchem.com	PROPN
eurjchem-1477	1	53	eaton	eaton	PROPN
eurjchem-1477	1	54	’s	’s	PART
eurjchem-1477	1	55	reagent	reagent	ADJ
eurjchem-1477	1	56	catalysed	catalyse	VERB
eurjchem-1477	1	57	alacritous	alacritous	ADJ
eurjchem-1477	1	58	synthesis	synthesis	NOUN
eurjchem-1477	1	59	of	of	ADP
eurjchem-1477	1	60	3‐benzazepinones	3‐benzazepinones	NUM
eurjchem-1477	1	61	shubhavathi	shubhavathi	NOUN
eurjchem-1477	1	62	thimmaiah	thimmaiah	PROPN
eurjchem-1477	1	63	1	1	NUM
eurjchem-1477	1	64	,	,	PUNCT
eurjchem-1477	1	65	mallesha	mallesha	PROPN
eurjchem-1477	1	66	ningegowda	ningegowda	PROPN
eurjchem-1477	1	67	2	2	NUM
eurjchem-1477	1	68	,	,	PUNCT
eurjchem-1477	1	69	nanjunda	nanjunda	ADJ
eurjchem-1477	1	70	swamy	swamy	PROPN
eurjchem-1477	1	71	shivananju	shivananju	PROPN
eurjchem-1477	1	72	3	3	NUM
eurjchem-1477	1	73	,	,	PUNCT
eurjchem-1477	1	74	raghu	raghu	PROPN
eurjchem-1477	1	75	ningegowda	ningegowda	PROPN
eurjchem-1477	1	76	1	1	NUM
eurjchem-1477	1	77	,	,	PUNCT
eurjchem-1477	1	78	ranjith	ranjith	PROPN
eurjchem-1477	1	79	siddaraj	siddaraj	ADJ
eurjchem-1477	1	80	1	1	NUM
eurjchem-1477	1	81	and	and	CCONJ
eurjchem-1477	1	82	babu	babu	PROPN
eurjchem-1477	1	83	shubha	shubha	PROPN
eurjchem-1477	1	84	priya	priya	PROPN
eurjchem-1477	1	85	1	1	NUM
eurjchem-1477	1	86	,	,	PUNCT
eurjchem-1477	1	87	*	*	PROPN
eurjchem-1477	1	88	1	1	NUM
eurjchem-1477	1	89	department	department	NOUN
eurjchem-1477	1	90	of	of	ADP
eurjchem-1477	1	91	studies	study	NOUN
eurjchem-1477	1	92	in	in	ADP
eurjchem-1477	1	93	chemistry	chemistry	NOUN
eurjchem-1477	1	94	,	,	PUNCT
eurjchem-1477	1	95	university	university	NOUN
eurjchem-1477	1	96	of	of	ADP
eurjchem-1477	1	97	mysore	mysore	PROPN
eurjchem-1477	1	98	,	,	PUNCT
eurjchem-1477	1	99	manasagangotri	manasagangotri	NOUN
eurjchem-1477	1	100	,	,	PUNCT
eurjchem-1477	1	101	mysuru	mysuru	NOUN
eurjchem-1477	1	102	,	,	PUNCT
eurjchem-1477	1	103	570006	570006	NUM
eurjchem-1477	1	104	,	,	PUNCT
eurjchem-1477	1	105	karnataka	karnataka	PROPN
eurjchem-1477	1	106	,	,	PUNCT
eurjchem-1477	1	107	india	india	PROPN
eurjchem-1477	1	108	2	2	NUM
eurjchem-1477	1	109	research	research	NOUN
eurjchem-1477	1	110	and	and	CCONJ
eurjchem-1477	1	111	development	development	NOUN
eurjchem-1477	1	112	centre	centre	NOUN
eurjchem-1477	1	113	,	,	PUNCT
eurjchem-1477	1	114	chethan	chethan	PROPN
eurjchem-1477	1	115	joshi	joshi	PROPN
eurjchem-1477	1	116	exports	exports	PROPN
eurjchem-1477	1	117	biochem	biochem	PROPN
eurjchem-1477	1	118	pvt	pvt	PROPN
eurjchem-1477	1	119	.	.	PROPN
eurjchem-1477	1	120	ltd	ltd	PROPN
eurjchem-1477	1	121	.	.	PROPN
eurjchem-1477	1	122	,	,	PUNCT
eurjchem-1477	1	123	bommanahalli	bommanahalli	PROPN
eurjchem-1477	1	124	,	,	PUNCT
eurjchem-1477	1	125	bangalore	bangalore	NOUN
eurjchem-1477	1	126	,	,	PUNCT
eurjchem-1477	1	127	560068	560068	NUM
eurjchem-1477	1	128	,	,	PUNCT
eurjchem-1477	1	129	india	india	PROPN
eurjchem-1477	1	130	3	3	PROPN
eurjchem-1477	1	131	department	department	PROPN
eurjchem-1477	1	132	of	of	ADP
eurjchem-1477	1	133	biotechnology	biotechnology	NOUN
eurjchem-1477	1	134	,	,	PUNCT
eurjchem-1477	1	135	jss	jss	PROPN
eurjchem-1477	1	136	science	science	PROPN
eurjchem-1477	1	137	and	and	CCONJ
eurjchem-1477	1	138	technology	technology	PROPN
eurjchem-1477	1	139	university	university	PROPN
eurjchem-1477	1	140	,	,	PUNCT
eurjchem-1477	1	141	jss	jss	PROPN
eurjchem-1477	1	142	technical	technical	PROPN
eurjchem-1477	1	143	institutions	institutions	PROPN
eurjchem-1477	1	144	campus	campus	PROPN
eurjchem-1477	1	145	,	,	PUNCT
eurjchem-1477	1	146	mysuru	mysuru	NOUN
eurjchem-1477	1	147	,	,	PUNCT
eurjchem-1477	1	148	570006	570006	NUM
eurjchem-1477	1	149	,	,	PUNCT
eurjchem-1477	1	150	karnataka	karnataka	PROPN
eurjchem-1477	1	151	,	,	PUNCT
eurjchem-1477	1	152	india	india	PROPN
eurjchem-1477	1	153	*	*	PUNCT
eurjchem-1477	1	154	corresponding	correspond	VERB
eurjchem-1477	1	155	author	author	NOUN
eurjchem-1477	1	156	at	at	ADP
eurjchem-1477	1	157	:	:	PUNCT
eurjchem-1477	1	158	department	department	NOUN
eurjchem-1477	1	159	of	of	ADP
eurjchem-1477	1	160	studies	study	NOUN
eurjchem-1477	1	161	in	in	ADP
eurjchem-1477	1	162	chemistry	chemistry	NOUN
eurjchem-1477	1	163	,	,	PUNCT
eurjchem-1477	1	164	university	university	NOUN
eurjchem-1477	1	165	of	of	ADP
eurjchem-1477	1	166	mysore	mysore	PROPN
eurjchem-1477	1	167	,	,	PUNCT
eurjchem-1477	1	168	manasagangotri	manasagangotri	NOUN
eurjchem-1477	1	169	,	,	PUNCT
eurjchem-1477	1	170	mysuru	mysuru	NOUN
eurjchem-1477	1	171	,	,	PUNCT
eurjchem-1477	1	172	570006	570006	NUM
eurjchem-1477	1	173	,	,	PUNCT
eurjchem-1477	1	174	karnataka	karnataka	PROPN
eurjchem-1477	1	175	,	,	PUNCT
eurjchem-1477	1	176	india	india	PROPN
eurjchem-1477	1	177	.	.	PUNCT
eurjchem-1477	2	1	tel	tel	PROPN
eurjchem-1477	2	2	.	.	PUNCT
eurjchem-1477	2	3	:	:	PUNCT
eurjchem-1477	3	1	+91.821.2419448	+91.821.2419448	X
eurjchem-1477	3	2	.	.	PUNCT
eurjchem-1477	3	3	fax	fax	NOUN
eurjchem-1477	3	4	:	:	PUNCT
eurjchem-1477	3	5	+91.821.2419363	+91.821.2419363	PROPN
eurjchem-1477	3	6	.	.	PUNCT
eurjchem-1477	3	7	e‐mail	e‐mail	PUNCT
eurjchem-1477	4	1	address	address	NOUN
eurjchem-1477	4	2	:	:	PUNCT
eurjchem-1477	4	3	priyabs_chem@yahoo.com	priyabs_chem@yahoo.com	X
eurjchem-1477	4	4	(	(	PUNCT
eurjchem-1477	4	5	b.s	b.s	PROPN
eurjchem-1477	4	6	.	.	PROPN
eurjchem-1477	4	7	priya	priya	PROPN
eurjchem-1477	4	8	)	)	PUNCT
eurjchem-1477	4	9	.	.	PUNCT
eurjchem-1477	5	1	article	article	NOUN
eurjchem-1477	5	2	information	information	PROPN
eurjchem-1477	5	3	abstract	abstract	ADJ
eurjchem-1477	5	4	doi	doi	PROPN
eurjchem-1477	5	5	:	:	PUNCT
eurjchem-1477	5	6	 	 	SPACE
eurjchem-1477	5	7	10.5155	10.5155	NUM
eurjchem-1477	5	8	/	/	SYM
eurjchem-1477	5	9	eurjchem.7.4.391	eurjchem.7.4.391	PROPN
eurjchem-1477	5	10	-	-	SYM
eurjchem-1477	5	11	396.1477	396.1477	NUM
eurjchem-1477	5	12	received	receive	VERB
eurjchem-1477	5	13	:	:	PUNCT
eurjchem-1477	5	14	13	13	NUM
eurjchem-1477	5	15	july	july	PROPN
eurjchem-1477	5	16	2016	2016	NUM
eurjchem-1477	5	17	accepted	accept	VERB
eurjchem-1477	5	18	:	:	PUNCT
eurjchem-1477	5	19	07	07	NUM
eurjchem-1477	5	20	august	august	PROPN
eurjchem-1477	5	21	2016	2016	NUM
eurjchem-1477	5	22	published	publish	VERB
eurjchem-1477	5	23	online	online	ADV
eurjchem-1477	5	24	:	:	PUNCT
eurjchem-1477	5	25	31	31	NUM
eurjchem-1477	5	26	december	december	PROPN
eurjchem-1477	5	27	2016	2016	NUM
eurjchem-1477	5	28	printed	print	VERB
eurjchem-1477	5	29	:	:	PUNCT
eurjchem-1477	5	30	31	31	NUM
eurjchem-1477	5	31	december	december	PROPN
eurjchem-1477	5	32	2016	2016	NUM
eurjchem-1477	5	33	  	  	SPACE
eurjchem-1477	5	34	an	an	DET
eurjchem-1477	5	35	expeditious	expeditious	ADJ
eurjchem-1477	5	36	method	method	NOUN
eurjchem-1477	5	37	for	for	ADP
eurjchem-1477	5	38	the	the	DET
eurjchem-1477	5	39	synthesis	synthesis	NOUN
eurjchem-1477	5	40	of	of	ADP
eurjchem-1477	5	41	3‐benzazepinones	3‐benzazepinone	NOUN
eurjchem-1477	5	42	has	have	AUX
eurjchem-1477	5	43	been	be	AUX
eurjchem-1477	5	44	developed	develop	VERB
eurjchem-1477	5	45	by	by	ADP
eurjchem-1477	5	46	using	use	VERB
eurjchem-1477	5	47	a	a	DET
eurjchem-1477	5	48	mixture	mixture	NOUN
eurjchem-1477	5	49	of	of	ADP
eurjchem-1477	5	50	phosphorus	phosphorus	NOUN
eurjchem-1477	5	51	pentoxide‐methane	pentoxide‐methane	NOUN
eurjchem-1477	5	52	sulfonic	sulfonic	ADJ
eurjchem-1477	5	53	acid	acid	NOUN
eurjchem-1477	5	54	(	(	PUNCT
eurjchem-1477	5	55	eaton	eaton	PROPN
eurjchem-1477	5	56	’s	’s	PART
eurjchem-1477	5	57	reagent	reagent	NOUN
eurjchem-1477	5	58	)	)	PUNCT
eurjchem-1477	5	59	at	at	ADP
eurjchem-1477	5	60	room	room	NOUN
eurjchem-1477	5	61	temperature	temperature	NOUN
eurjchem-1477	5	62	under	under	ADP
eurjchem-1477	5	63	solvent	solvent	NOUN
eurjchem-1477	5	64	and	and	CCONJ
eurjchem-1477	5	65	metal	metal	NOUN
eurjchem-1477	5	66	catalyst	catalyst	NOUN
eurjchem-1477	5	67	free	free	ADJ
eurjchem-1477	5	68	condition	condition	NOUN
eurjchem-1477	5	69	.	.	PUNCT
eurjchem-1477	6	1	wide	wide	ADJ
eurjchem-1477	6	2	functional	functional	ADJ
eurjchem-1477	6	3	group	group	NOUN
eurjchem-1477	6	4	tolerance	tolerance	NOUN
eurjchem-1477	6	5	,	,	PUNCT
eurjchem-1477	6	6	mild	mild	ADJ
eurjchem-1477	6	7	reaction	reaction	NOUN
eurjchem-1477	6	8	conditions	condition	NOUN
eurjchem-1477	6	9	,	,	PUNCT
eurjchem-1477	6	10	simple	simple	ADJ
eurjchem-1477	6	11	procedure	procedure	NOUN
eurjchem-1477	6	12	,	,	PUNCT
eurjchem-1477	6	13	ease	ease	NOUN
eurjchem-1477	6	14	of	of	ADP
eurjchem-1477	6	15	work‐up	work‐up	PUNCT
eurjchem-1477	6	16	and	and	CCONJ
eurjchem-1477	6	17	high	high	ADJ
eurjchem-1477	6	18	yields	yield	NOUN
eurjchem-1477	6	19	is	be	AUX
eurjchem-1477	6	20	the	the	DET
eurjchem-1477	6	21	citable	citable	ADJ
eurjchem-1477	6	22	features	feature	NOUN
eurjchem-1477	6	23	of	of	ADP
eurjchem-1477	6	24	this	this	DET
eurjchem-1477	6	25	protocol	protocol	NOUN
eurjchem-1477	6	26	.	.	PUNCT
eurjchem-1477	7	1	keywords	keyword	VERB
eurjchem-1477	7	2	alacritous	alacritous	PROPN
eurjchem-1477	7	3	eaton	eaton	PROPN
eurjchem-1477	7	4	’s	’s	PART
eurjchem-1477	7	5	reagent	reagent	ADJ
eurjchem-1477	7	6	3‐benzazepinone	3‐benzazepinone	NUM
eurjchem-1477	7	7	solvent	solvent	ADJ
eurjchem-1477	7	8	free	free	ADJ
eurjchem-1477	7	9	reaction	reaction	NOUN
eurjchem-1477	7	10	methane	methane	NOUN
eurjchem-1477	7	11	sulfonic	sulfonic	ADJ
eurjchem-1477	7	12	acid	acid	NOUN
eurjchem-1477	7	13	phosphorous	phosphorous	ADJ
eurjchem-1477	7	14	pentoxide	pentoxide	NOUN
eurjchem-1477	7	15	cite	cite	VERB
eurjchem-1477	7	16	this	this	PRON
eurjchem-1477	7	17	:	:	PUNCT
eurjchem-1477	7	18	eur	eur	PROPN
eurjchem-1477	7	19	.	.	PUNCT
eurjchem-1477	8	1	j.	j.	PROPN
eurjchem-1477	8	2	chem	chem	PROPN
eurjchem-1477	8	3	.	.	PUNCT
eurjchem-1477	9	1	2016	2016	NUM
eurjchem-1477	9	2	,	,	PUNCT
eurjchem-1477	9	3	7(4	7(4	NUM
eurjchem-1477	9	4	)	)	PUNCT
eurjchem-1477	9	5	,	,	PUNCT
eurjchem-1477	9	6	391‐396	391‐396	NUM
eurjchem-1477	9	7	1	1	NUM
eurjchem-1477	9	8	.	.	PUNCT
eurjchem-1477	10	1	introduction	introduction	NOUN
eurjchem-1477	10	2	heterocyclic	heterocyclic	ADJ
eurjchem-1477	10	3	compounds	compound	NOUN
eurjchem-1477	10	4	have	have	AUX
eurjchem-1477	10	5	gained	gain	VERB
eurjchem-1477	10	6	more	more	ADJ
eurjchem-1477	10	7	importance	importance	NOUN
eurjchem-1477	10	8	because	because	SCONJ
eurjchem-1477	10	9	of	of	ADP
eurjchem-1477	10	10	their	their	PRON
eurjchem-1477	10	11	versatile	versatile	ADJ
eurjchem-1477	10	12	role	role	NOUN
eurjchem-1477	10	13	in	in	ADP
eurjchem-1477	10	14	the	the	DET
eurjchem-1477	10	15	biological	biological	ADJ
eurjchem-1477	10	16	field	field	NOUN
eurjchem-1477	10	17	.	.	PUNCT
eurjchem-1477	11	1	among	among	ADP
eurjchem-1477	11	2	various	various	ADJ
eurjchem-1477	11	3	heterocycles	heterocycle	NOUN
eurjchem-1477	11	4	,	,	PUNCT
eurjchem-1477	11	5	seven	seven	NUM
eurjchem-1477	11	6	membered	membere	VERB
eurjchem-1477	11	7	nitrogen	nitrogen	NOUN
eurjchem-1477	11	8	containing	contain	VERB
eurjchem-1477	11	9	heterocyclic	heterocyclic	ADJ
eurjchem-1477	11	10	compounds	compound	NOUN
eurjchem-1477	11	11	,	,	PUNCT
eurjchem-1477	11	12	in	in	ADP
eurjchem-1477	11	13	particularly	particularly	ADV
eurjchem-1477	11	14	,	,	PUNCT
eurjchem-1477	11	15	3‐benzazepinones	3‐benzazepinone	NOUN
eurjchem-1477	11	16	have	have	AUX
eurjchem-1477	11	17	received	receive	VERB
eurjchem-1477	11	18	considerable	considerable	ADJ
eurjchem-1477	11	19	attention	attention	NOUN
eurjchem-1477	11	20	in	in	ADP
eurjchem-1477	11	21	the	the	DET
eurjchem-1477	11	22	view	view	NOUN
eurjchem-1477	11	23	of	of	ADP
eurjchem-1477	11	24	its	its	PRON
eurjchem-1477	11	25	diverse	diverse	ADJ
eurjchem-1477	11	26	biological	biological	ADJ
eurjchem-1477	11	27	importance	importance	NOUN
eurjchem-1477	11	28	for	for	ADP
eurjchem-1477	11	29	example	example	NOUN
eurjchem-1477	11	30	as	as	ADP
eurjchem-1477	11	31	γ‐secretase	γ‐secretase	PUNCT
eurjchem-1477	11	32	inhibitors	inhibitor	NOUN
eurjchem-1477	11	33	[	[	X
eurjchem-1477	11	34	1	1	NUM
eurjchem-1477	11	35	]	]	PUNCT
eurjchem-1477	11	36	,	,	PUNCT
eurjchem-1477	11	37	bradycardia	bradycardia	ADJ
eurjchem-1477	11	38	agents	agent	NOUN
eurjchem-1477	12	1	[	[	X
eurjchem-1477	12	2	2	2	NUM
eurjchem-1477	12	3	]	]	PUNCT
eurjchem-1477	12	4	and	and	CCONJ
eurjchem-1477	12	5	it	it	PRON
eurjchem-1477	12	6	also	also	ADV
eurjchem-1477	12	7	serves	serve	VERB
eurjchem-1477	12	8	as	as	ADP
eurjchem-1477	12	9	remedies	remedy	NOUN
eurjchem-1477	12	10	to	to	ADP
eurjchem-1477	12	11	several	several	ADJ
eurjchem-1477	12	12	diseases	disease	NOUN
eurjchem-1477	12	13	like	like	ADP
eurjchem-1477	12	14	parkinson	parkinson	NOUN
eurjchem-1477	12	15	’s	’s	PART
eurjchem-1477	12	16	,	,	PUNCT
eurjchem-1477	12	17	cancer	cancer	NOUN
eurjchem-1477	12	18	,	,	PUNCT
eurjchem-1477	12	19	pain	pain	NOUN
eurjchem-1477	12	20	and	and	CCONJ
eurjchem-1477	12	21	cardiovas‐	cardiovas‐	NOUN
eurjchem-1477	13	1	cular	cular	ADJ
eurjchem-1477	13	2	[	[	X
eurjchem-1477	13	3	3‐8	3‐8	NOUN
eurjchem-1477	13	4	]	]	X
eurjchem-1477	13	5	.	.	PUNCT
eurjchem-1477	14	1	because	because	SCONJ
eurjchem-1477	14	2	of	of	ADP
eurjchem-1477	14	3	its	its	PRON
eurjchem-1477	14	4	broad	broad	ADJ
eurjchem-1477	14	5	biological	biological	ADJ
eurjchem-1477	14	6	importance	importance	NOUN
eurjchem-1477	14	7	,	,	PUNCT
eurjchem-1477	14	8	many	many	ADJ
eurjchem-1477	14	9	synthetic	synthetic	ADJ
eurjchem-1477	14	10	efforts	effort	NOUN
eurjchem-1477	14	11	have	have	AUX
eurjchem-1477	14	12	been	be	AUX
eurjchem-1477	14	13	made	make	VERB
eurjchem-1477	14	14	to	to	PART
eurjchem-1477	14	15	construct	construct	VERB
eurjchem-1477	14	16	this	this	DET
eurjchem-1477	14	17	motif	motif	NOUN
eurjchem-1477	14	18	.	.	PUNCT
eurjchem-1477	15	1	among	among	ADP
eurjchem-1477	15	2	these	these	DET
eurjchem-1477	15	3	widely	widely	ADV
eurjchem-1477	15	4	employed	employ	VERB
eurjchem-1477	15	5	methods	method	NOUN
eurjchem-1477	15	6	are	be	AUX
eurjchem-1477	15	7	intramolecular	intramolecular	ADJ
eurjchem-1477	15	8	hydroamidation	hydroamidation	NOUN
eurjchem-1477	15	9	of	of	ADP
eurjchem-1477	15	10	2‐(1‐alkylnyl	2‐(1‐alkylnyl	NUM
eurjchem-1477	15	11	)	)	PUNCT
eurjchem-1477	15	12	phenylacetamide	phenylacetamide	ADV
eurjchem-1477	15	13	[	[	X
eurjchem-1477	15	14	9	9	NUM
eurjchem-1477	15	15	]	]	PUNCT
eurjchem-1477	15	16	,	,	PUNCT
eurjchem-1477	15	17	intra‐	intra‐	PROPN
eurjchem-1477	15	18	molecular	molecular	ADJ
eurjchem-1477	15	19	friedel‐crafts	friedel‐craft	NOUN
eurjchem-1477	15	20	cyclization	cyclization	NOUN
eurjchem-1477	15	21	of	of	ADP
eurjchem-1477	15	22	n‐chloro	n‐chloro	PUNCT
eurjchem-1477	15	23	acetyl‐n‐	acetyl‐n‐	PROPN
eurjchem-1477	15	24	methyl	methyl	PROPN
eurjchem-1477	15	25	phenethyl	phenethyl	PROPN
eurjchem-1477	15	26	amine	amine	PROPN
eurjchem-1477	15	27	[	[	X
eurjchem-1477	15	28	10	10	NUM
eurjchem-1477	15	29	]	]	PUNCT
eurjchem-1477	15	30	,	,	PUNCT
eurjchem-1477	15	31	inter	inter	ADJ
eurjchem-1477	15	32	or	or	CCONJ
eurjchem-1477	15	33	intra‐molecular	intra‐molecular	ADJ
eurjchem-1477	15	34	conden‐	conden‐	NOUN
eurjchem-1477	15	35	sation	sation	NOUN
eurjchem-1477	15	36	of	of	ADP
eurjchem-1477	15	37	ƹ‐oxo	ƹ‐oxo	NOUN
eurjchem-1477	15	38	acids	acid	NOUN
eurjchem-1477	15	39	with	with	ADP
eurjchem-1477	15	40	ammonium	ammonium	NOUN
eurjchem-1477	15	41	acetate	acetate	NOUN
eurjchem-1477	15	42	and	and	CCONJ
eurjchem-1477	15	43	2‐(2‐	2‐(2‐	PROPN
eurjchem-1477	15	44	oxoalkyl)phenylacetic	oxoalkyl)phenylacetic	ADJ
eurjchem-1477	15	45	acid	acid	NOUN
eurjchem-1477	15	46	with	with	ADP
eurjchem-1477	15	47	phenylglycinol	phenylglycinol	ADJ
eurjchem-1477	15	48	[	[	X
eurjchem-1477	15	49	11	11	NUM
eurjchem-1477	15	50	]	]	PUNCT
eurjchem-1477	15	51	,	,	PUNCT
eurjchem-1477	15	52	micro‐	micro‐	PRON
eurjchem-1477	15	53	wave	wave	VERB
eurjchem-1477	15	54	assisted	assist	VERB
eurjchem-1477	15	55	condensation	condensation	NOUN
eurjchem-1477	15	56	of	of	ADP
eurjchem-1477	15	57	primary	primary	ADJ
eurjchem-1477	15	58	amines	amine	NOUN
eurjchem-1477	15	59	with	with	ADP
eurjchem-1477	15	60	keto	keto	NOUN
eurjchem-1477	15	61	acids	acid	NOUN
eurjchem-1477	16	1	[	[	X
eurjchem-1477	16	2	12	12	NUM
eurjchem-1477	16	3	]	]	PUNCT
eurjchem-1477	16	4	.	.	PUNCT
eurjchem-1477	17	1	many	many	ADJ
eurjchem-1477	17	2	acid	acid	ADJ
eurjchem-1477	17	3	and	and	CCONJ
eurjchem-1477	17	4	metal	metal	NOUN
eurjchem-1477	17	5	catalysed	catalyse	VERB
eurjchem-1477	17	6	methods	method	NOUN
eurjchem-1477	17	7	are	be	AUX
eurjchem-1477	17	8	also	also	ADV
eurjchem-1477	17	9	well	well	ADV
eurjchem-1477	17	10	documented	document	VERB
eurjchem-1477	17	11	in	in	ADP
eurjchem-1477	17	12	the	the	DET
eurjchem-1477	17	13	literature	literature	NOUN
eurjchem-1477	17	14	which	which	PRON
eurjchem-1477	17	15	include	include	VERB
eurjchem-1477	17	16	conc	conc	NOUN
eurjchem-1477	17	17	.	.	PUNCT
eurjchem-1477	18	1	hcl/	hcl/	PROPN
eurjchem-1477	18	2	ch3cooh	ch3cooh	PUNCT
eurjchem-1477	19	1	[	[	X
eurjchem-1477	19	2	13	13	NUM
eurjchem-1477	19	3	]	]	PUNCT
eurjchem-1477	19	4	,	,	PUNCT
eurjchem-1477	19	5	au(pph3)cl	au(pph3)cl	NOUN
eurjchem-1477	19	6	/	/	SYM
eurjchem-1477	19	7	agsbf6	agsbf6	PROPN
eurjchem-1477	19	8	and	and	CCONJ
eurjchem-1477	19	9	aubr3	aubr3	PROPN
eurjchem-1477	19	10	/	/	SYM
eurjchem-1477	19	11	ch3cooh	ch3cooh	PUNCT
eurjchem-1477	20	1	[	[	X
eurjchem-1477	20	2	9	9	NUM
eurjchem-1477	20	3	]	]	PUNCT
eurjchem-1477	20	4	,	,	PUNCT
eurjchem-1477	20	5	pd(oac)2(pph3)2	pd(oac)2(pph3)2	NOUN
eurjchem-1477	20	6	/	/	SYM
eurjchem-1477	20	7	dmf	dmf	PROPN
eurjchem-1477	21	1	[	[	X
eurjchem-1477	21	2	9	9	NUM
eurjchem-1477	21	3	]	]	PUNCT
eurjchem-1477	21	4	,	,	PUNCT
eurjchem-1477	21	5	nh4oac	nh4oac	PROPN
eurjchem-1477	21	6	/	/	SYM
eurjchem-1477	21	7	ch3cooh	ch3cooh	PUNCT
eurjchem-1477	22	1	[	[	X
eurjchem-1477	22	2	11	11	NUM
eurjchem-1477	22	3	]	]	PUNCT
eurjchem-1477	22	4	.	.	PUNCT
eurjchem-1477	23	1	in	in	ADP
eurjchem-1477	23	2	addition	addition	NOUN
eurjchem-1477	23	3	to	to	ADP
eurjchem-1477	23	4	this	this	PRON
eurjchem-1477	23	5	,	,	PUNCT
eurjchem-1477	23	6	3‐benzazepinones	3‐benzazepinone	NOUN
eurjchem-1477	23	7	were	be	AUX
eurjchem-1477	23	8	obtained	obtain	VERB
eurjchem-1477	23	9	as	as	ADP
eurjchem-1477	23	10	by	by	ADP
eurjchem-1477	23	11	product	product	NOUN
eurjchem-1477	23	12	during	during	ADP
eurjchem-1477	23	13	the	the	DET
eurjchem-1477	23	14	synthesis	synthesis	NOUN
eurjchem-1477	23	15	of	of	ADP
eurjchem-1477	23	16	fully	fully	ADV
eurjchem-1477	23	17	conjugated	conjugate	VERB
eurjchem-1477	23	18	seven	seven	NUM
eurjchem-1477	23	19	/	/	SYM
eurjchem-1477	23	20	eight	eight	NUM
eurjchem-1477	23	21	membered	membere	VERB
eurjchem-1477	23	22	heterocyclic	heterocyclic	NOUN
eurjchem-1477	23	23	systems	system	NOUN
eurjchem-1477	23	24	[	[	X
eurjchem-1477	23	25	14	14	NUM
eurjchem-1477	23	26	]	]	PUNCT
eurjchem-1477	23	27	.	.	PUNCT
eurjchem-1477	24	1	however	however	ADV
eurjchem-1477	24	2	,	,	PUNCT
eurjchem-1477	24	3	most	most	ADJ
eurjchem-1477	24	4	of	of	ADP
eurjchem-1477	24	5	the	the	DET
eurjchem-1477	24	6	above	above	ADJ
eurjchem-1477	24	7	described	describe	VERB
eurjchem-1477	24	8	protocols	protocol	NOUN
eurjchem-1477	24	9	suffers	suffer	VERB
eurjchem-1477	24	10	from	from	ADP
eurjchem-1477	24	11	serious	serious	ADJ
eurjchem-1477	24	12	drawbacks	drawback	NOUN
eurjchem-1477	24	13	such	such	ADJ
eurjchem-1477	24	14	as	as	ADP
eurjchem-1477	24	15	tedious	tedious	ADJ
eurjchem-1477	24	16	workup	workup	NOUN
eurjchem-1477	24	17	,	,	PUNCT
eurjchem-1477	24	18	prolonged	prolonged	ADJ
eurjchem-1477	24	19	reaction	reaction	NOUN
eurjchem-1477	24	20	time	time	NOUN
eurjchem-1477	24	21	,	,	PUNCT
eurjchem-1477	24	22	expensive	expensive	ADJ
eurjchem-1477	24	23	reagents	reagent	NOUN
eurjchem-1477	24	24	or	or	CCONJ
eurjchem-1477	24	25	catalysts	catalyst	NOUN
eurjchem-1477	24	26	,	,	PUNCT
eurjchem-1477	24	27	high	high	ADJ
eurjchem-1477	24	28	reaction	reaction	NOUN
eurjchem-1477	24	29	temperature	temperature	NOUN
eurjchem-1477	24	30	and	and	CCONJ
eurjchem-1477	24	31	even	even	ADV
eurjchem-1477	24	32	then	then	ADV
eurjchem-1477	24	33	yields	yield	NOUN
eurjchem-1477	24	34	are	be	AUX
eurjchem-1477	24	35	not	not	PART
eurjchem-1477	24	36	competent	competent	ADJ
eurjchem-1477	24	37	.	.	PUNCT
eurjchem-1477	25	1	in	in	ADP
eurjchem-1477	25	2	this	this	DET
eurjchem-1477	25	3	connection	connection	NOUN
eurjchem-1477	25	4	,	,	PUNCT
eurjchem-1477	25	5	we	we	PRON
eurjchem-1477	25	6	have	have	AUX
eurjchem-1477	25	7	developed	develop	VERB
eurjchem-1477	25	8	a	a	DET
eurjchem-1477	25	9	protocol	protocol	NOUN
eurjchem-1477	25	10	which	which	PRON
eurjchem-1477	25	11	circumvents	circumvent	VERB
eurjchem-1477	25	12	these	these	DET
eurjchem-1477	25	13	demerits	demerit	NOUN
eurjchem-1477	25	14	.	.	PUNCT
eurjchem-1477	26	1	in	in	ADP
eurjchem-1477	26	2	this	this	DET
eurjchem-1477	26	3	communication	communication	NOUN
eurjchem-1477	26	4	,	,	PUNCT
eurjchem-1477	26	5	we	we	PRON
eurjchem-1477	26	6	report	report	VERB
eurjchem-1477	26	7	the	the	DET
eurjchem-1477	26	8	synthesis	synthesis	NOUN
eurjchem-1477	26	9	of	of	ADP
eurjchem-1477	26	10	3‐benzazepinones	3‐benzazepinone	NOUN
eurjchem-1477	26	11	by	by	ADP
eurjchem-1477	26	12	using	use	VERB
eurjchem-1477	26	13	eaton	eaton	PROPN
eurjchem-1477	26	14	’s	’s	PART
eurjchem-1477	26	15	reagent	reagent	NOUN
eurjchem-1477	26	16	.	.	PUNCT
eurjchem-1477	27	1	eaton	eaton	PROPN
eurjchem-1477	27	2	’s	’s	PART
eurjchem-1477	27	3	reagent	reagent	NOUN
eurjchem-1477	27	4	(	(	PUNCT
eurjchem-1477	27	5	1:10	1:10	NUM
eurjchem-1477	27	6	,	,	PUNCT
eurjchem-1477	27	7	phosphorus	phosphorus	NOUN
eurjchem-1477	27	8	pentoxide	pentoxide	NOUN
eurjchem-1477	27	9	in	in	ADP
eurjchem-1477	27	10	methane	methane	NOUN
eurjchem-1477	27	11	sulfonic	sulfonic	ADJ
eurjchem-1477	27	12	acid	acid	NOUN
eurjchem-1477	27	13	)	)	PUNCT
eurjchem-1477	27	14	is	be	AUX
eurjchem-1477	27	15	a	a	DET
eurjchem-1477	27	16	commercially	commercially	ADV
eurjchem-1477	27	17	available	available	ADJ
eurjchem-1477	27	18	inexpensive	inexpensive	ADJ
eurjchem-1477	27	19	,	,	PUNCT
eurjchem-1477	27	20	low	low	ADJ
eurjchem-1477	27	21	viscous	viscous	ADJ
eurjchem-1477	27	22	,	,	PUNCT
eurjchem-1477	27	23	easy	easy	ADJ
eurjchem-1477	27	24	to	to	PART
eurjchem-1477	27	25	handle	handle	VERB
eurjchem-1477	27	26	reagent	reagent	NOUN
eurjchem-1477	27	27	and	and	CCONJ
eurjchem-1477	27	28	found	find	VERB
eurjchem-1477	27	29	to	to	PART
eurjchem-1477	27	30	be	be	AUX
eurjchem-1477	27	31	a	a	DET
eurjchem-1477	27	32	good	good	ADJ
eurjchem-1477	27	33	alter‐	alter‐	NOUN
eurjchem-1477	27	34	native	native	ADJ
eurjchem-1477	27	35	to	to	ADP
eurjchem-1477	27	36	polyphosphoric	polyphosphoric	ADJ
eurjchem-1477	27	37	acid	acid	NOUN
eurjchem-1477	27	38	because	because	SCONJ
eurjchem-1477	27	39	of	of	ADP
eurjchem-1477	27	40	its	its	PRON
eurjchem-1477	27	41	eco‐friendly	eco‐friendly	ADV
eurjchem-1477	27	42	nature	nature	NOUN
eurjchem-1477	27	43	[	[	X
eurjchem-1477	27	44	15	15	NUM
eurjchem-1477	27	45	]	]	X
eurjchem-1477	27	46	,	,	PUNCT
eurjchem-1477	27	47	shorter	short	ADJ
eurjchem-1477	27	48	reaction	reaction	NOUN
eurjchem-1477	27	49	time	time	NOUN
eurjchem-1477	27	50	,	,	PUNCT
eurjchem-1477	27	51	no	no	DET
eurjchem-1477	27	52	additional	additional	ADJ
eurjchem-1477	27	53	solvent	solvent	NOUN
eurjchem-1477	27	54	required	require	VERB
eurjchem-1477	27	55	,	,	PUNCT
eurjchem-1477	27	56	easier	easy	ADJ
eurjchem-1477	27	57	workup	workup	NOUN
eurjchem-1477	27	58	and	and	CCONJ
eurjchem-1477	27	59	products	product	NOUN
eurjchem-1477	27	60	with	with	ADP
eurjchem-1477	27	61	high	high	ADJ
eurjchem-1477	27	62	purity	purity	NOUN
eurjchem-1477	27	63	in	in	ADP
eurjchem-1477	27	64	a	a	DET
eurjchem-1477	27	65	good	good	NOUN
eurjchem-1477	27	66	to	to	ADP
eurjchem-1477	27	67	excellent	excellent	ADJ
eurjchem-1477	27	68	yields	yield	NOUN
eurjchem-1477	27	69	[	[	X
eurjchem-1477	27	70	16	16	NUM
eurjchem-1477	27	71	]	]	PUNCT
eurjchem-1477	27	72	.	.	PUNCT
eurjchem-1477	28	1	in	in	ADP
eurjchem-1477	28	2	the	the	DET
eurjchem-1477	28	3	recent	recent	ADJ
eurjchem-1477	28	4	literature	literature	NOUN
eurjchem-1477	28	5	,	,	PUNCT
eurjchem-1477	28	6	eaton	eaton	PROPN
eurjchem-1477	28	7	’s	’s	PART
eurjchem-1477	28	8	reagent	reagent	NOUN
eurjchem-1477	28	9	emerged	emerge	VERB
eurjchem-1477	28	10	as	as	ADP
eurjchem-1477	28	11	one	one	NUM
eurjchem-1477	28	12	of	of	ADP
eurjchem-1477	28	13	the	the	DET
eurjchem-1477	28	14	better	well	ADJ
eurjchem-1477	28	15	reagent	reagent	NOUN
eurjchem-1477	28	16	in	in	ADP
eurjchem-1477	28	17	organic	organic	ADJ
eurjchem-1477	28	18	synthesis	synthesis	NOUN
eurjchem-1477	28	19	for	for	ADP
eurjchem-1477	28	20	example	example	NOUN
eurjchem-1477	28	21	in	in	ADP
eurjchem-1477	28	22	the	the	DET
eurjchem-1477	28	23	synthesis	synthesis	NOUN
eurjchem-1477	28	24	of	of	ADP
eurjchem-1477	28	25	3,4‐dihydropyridin‐	3,4‐dihydropyridin‐	NUM
eurjchem-1477	28	26	2‐(1h)‐ones	2‐(1h)‐one	NOUN
eurjchem-1477	28	27	[	[	X
eurjchem-1477	28	28	17	17	NUM
eurjchem-1477	28	29	]	]	PUNCT
eurjchem-1477	28	30	,	,	PUNCT
eurjchem-1477	28	31	quinolones	quinolone	NOUN
eurjchem-1477	29	1	[	[	X
eurjchem-1477	29	2	18	18	NUM
eurjchem-1477	29	3	]	]	PUNCT
eurjchem-1477	29	4	,	,	PUNCT
eurjchem-1477	29	5	cardo	cardo	NOUN
eurjchem-1477	29	6	poly[benzimidazoles	poly[benzimidazole	NOUN
eurjchem-1477	29	7	]	]	PUNCT
eurjchem-1477	30	1	[	[	X
eurjchem-1477	30	2	19	19	NUM
eurjchem-1477	30	3	]	]	PUNCT
eurjchem-1477	30	4	,	,	PUNCT
eurjchem-1477	30	5	4‐hydroxycoumarin	4‐hydroxycoumarin	NOUN
eurjchem-1477	31	1	[	[	X
eurjchem-1477	31	2	20	20	NUM
eurjchem-1477	31	3	]	]	PUNCT
eurjchem-1477	31	4	,	,	PUNCT
eurjchem-1477	31	5	cyclopentanones	cyclopentanone	NOUN
eurjchem-1477	32	1	[	[	X
eurjchem-1477	32	2	21	21	NUM
eurjchem-1477	32	3	]	]	PUNCT
eurjchem-1477	32	4	,	,	PUNCT
eurjchem-1477	32	5	oxazole	oxazole	PROPN
eurjchem-1477	32	6	’s	’s	PART
eurjchem-1477	32	7	[	[	X
eurjchem-1477	32	8	22	22	NUM
eurjchem-1477	32	9	]	]	PUNCT
eurjchem-1477	32	10	,	,	PUNCT
eurjchem-1477	32	11	aryl	aryl	NOUN
eurjchem-1477	32	12	mesylates	mesylate	VERB
eurjchem-1477	32	13	[	[	X
eurjchem-1477	32	14	23	23	NUM
eurjchem-1477	32	15	]	]	PUNCT
eurjchem-1477	32	16	,	,	PUNCT
eurjchem-1477	32	17	chromones	chromone	NOUN
eurjchem-1477	32	18	and	and	CCONJ
eurjchem-1477	32	19	flavones	flavone	NOUN
eurjchem-1477	33	1	[	[	X
eurjchem-1477	33	2	24	24	NUM
eurjchem-1477	33	3	]	]	PUNCT
eurjchem-1477	33	4	,	,	PUNCT
eurjchem-1477	33	5	mono	mono	PROPN
eurjchem-1477	33	6	and	and	CCONJ
eurjchem-1477	33	7	bis‐chalcones	bis‐chalcone	NOUN
eurjchem-1477	34	1	[	[	X
eurjchem-1477	34	2	25	25	NUM
eurjchem-1477	34	3	]	]	PUNCT
eurjchem-1477	34	4	and	and	CCONJ
eurjchem-1477	34	5	bis(indolyl)methanes	bis(indolyl)methanes	NUM
eurjchem-1477	35	1	[	[	X
eurjchem-1477	35	2	26	26	NUM
eurjchem-1477	35	3	]	]	PUNCT
eurjchem-1477	35	4	.	.	PUNCT
eurjchem-1477	36	1	it	it	PRON
eurjchem-1477	36	2	is	be	AUX
eurjchem-1477	36	3	also	also	ADV
eurjchem-1477	36	4	used	use	VERB
eurjchem-1477	36	5	as	as	ADP
eurjchem-1477	36	6	catalyst	catalyst	NOUN
eurjchem-1477	36	7	for	for	ADP
eurjchem-1477	36	8	fisher‐indole	fisher‐indole	NOUN
eurjchem-1477	36	9	synthesis	synthesis	NOUN
eurjchem-1477	36	10	and	and	CCONJ
eurjchem-1477	36	11	beckmann	beckmann	NOUN
eurjchem-1477	36	12	rearrangement	rearrangement	PROPN
eurjchem-1477	36	13	process	process	NOUN
eurjchem-1477	36	14	[	[	X
eurjchem-1477	36	15	19	19	NUM
eurjchem-1477	36	16	]	]	PUNCT
eurjchem-1477	36	17	(	(	PUNCT
eurjchem-1477	36	18	figure	figure	NOUN
eurjchem-1477	36	19	1	1	NUM
eurjchem-1477	36	20	)	)	PUNCT
eurjchem-1477	36	21	.	.	PUNCT
eurjchem-1477	37	1	392	392	NUM
eurjchem-1477	37	2	thimmaiah	thimmaiah	PROPN
eurjchem-1477	37	3	et	et	PROPN
eurjchem-1477	37	4	al	al	PROPN
eurjchem-1477	37	5	.	.	PUNCT
eurjchem-1477	37	6	/	/	SYM
eurjchem-1477	37	7	european	european	PROPN
eurjchem-1477	37	8	journal	journal	PROPN
eurjchem-1477	37	9	of	of	ADP
eurjchem-1477	37	10	chemistry	chemistry	NOUN
eurjchem-1477	37	11	7	7	NUM
eurjchem-1477	37	12	(	(	PUNCT
eurjchem-1477	37	13	4	4	NUM
eurjchem-1477	37	14	)	)	PUNCT
eurjchem-1477	37	15	(	(	PUNCT
eurjchem-1477	37	16	2016	2016	NUM
eurjchem-1477	37	17	)	)	PUNCT
eurjchem-1477	37	18	391‐396	391‐396	NUM
eurjchem-1477	37	19	figure	figure	NOUN
eurjchem-1477	37	20	1	1	NUM
eurjchem-1477	37	21	.	.	PUNCT
eurjchem-1477	38	1	eaton	eaton	PROPN
eurjchem-1477	38	2	’s	’s	PART
eurjchem-1477	38	3	reagent	reagent	NOUN
eurjchem-1477	38	4	:	:	PUNCT
eurjchem-1477	38	5	a	a	DET
eurjchem-1477	38	6	common	common	ADJ
eurjchem-1477	38	7	reagent	reagent	NOUN
eurjchem-1477	38	8	in	in	ADP
eurjchem-1477	38	9	many	many	ADJ
eurjchem-1477	38	10	organic	organic	ADJ
eurjchem-1477	38	11	syntheses	synthesis	NOUN
eurjchem-1477	38	12	.	.	PUNCT
eurjchem-1477	39	1	2	2	X
eurjchem-1477	39	2	.	.	X
eurjchem-1477	39	3	experimental	experimental	ADJ
eurjchem-1477	39	4	2.1	2.1	NUM
eurjchem-1477	39	5	.	.	PUNCT
eurjchem-1477	39	6	material	material	NOUN
eurjchem-1477	39	7	and	and	CCONJ
eurjchem-1477	39	8	methods	methods	PROPN
eurjchem-1477	39	9	eaton	eaton	PROPN
eurjchem-1477	39	10	’s	’s	PART
eurjchem-1477	39	11	reagent	reagent	NOUN
eurjchem-1477	39	12	was	be	AUX
eurjchem-1477	39	13	purchased	purchase	VERB
eurjchem-1477	39	14	from	from	ADP
eurjchem-1477	39	15	sigma	sigma	PROPN
eurjchem-1477	39	16	aldrich	aldrich	PROPN
eurjchem-1477	39	17	co.	co.	PROPN
eurjchem-1477	39	18	,	,	PUNCT
eurjchem-1477	39	19	usa	usa	PROPN
eurjchem-1477	39	20	.	.	PROPN
eurjchem-1477	40	1	all	all	DET
eurjchem-1477	40	2	the	the	DET
eurjchem-1477	40	3	other	other	ADJ
eurjchem-1477	40	4	chemicals	chemical	NOUN
eurjchem-1477	40	5	and	and	CCONJ
eurjchem-1477	40	6	reagents	reagent	NOUN
eurjchem-1477	40	7	were	be	AUX
eurjchem-1477	40	8	purchased	purchase	VERB
eurjchem-1477	40	9	from	from	ADP
eurjchem-1477	40	10	merck	merck	NOUN
eurjchem-1477	40	11	chemicals	chemical	NOUN
eurjchem-1477	40	12	used	use	VERB
eurjchem-1477	40	13	without	without	ADP
eurjchem-1477	40	14	further	further	ADJ
eurjchem-1477	40	15	purifications	purification	NOUN
eurjchem-1477	40	16	.	.	PUNCT
eurjchem-1477	41	1	progress	progress	NOUN
eurjchem-1477	41	2	of	of	ADP
eurjchem-1477	41	3	the	the	DET
eurjchem-1477	41	4	reaction	reaction	NOUN
eurjchem-1477	41	5	were	be	AUX
eurjchem-1477	41	6	monitored	monitor	VERB
eurjchem-1477	41	7	by	by	ADP
eurjchem-1477	41	8	tlc	tlc	NOUN
eurjchem-1477	41	9	using	use	VERB
eurjchem-1477	41	10	ethyl	ethyl	PROPN
eurjchem-1477	41	11	acetate	acetate	NOUN
eurjchem-1477	41	12	:	:	PUNCT
eurjchem-1477	41	13	hexane	hexane	NOUN
eurjchem-1477	41	14	(	(	PUNCT
eurjchem-1477	41	15	1:1	1:1	NUM
eurjchem-1477	41	16	,	,	PUNCT
eurjchem-1477	41	17	v	v	NOUN
eurjchem-1477	41	18	:	:	PUNCT
eurjchem-1477	41	19	v	v	NOUN
eurjchem-1477	41	20	)	)	PUNCT
eurjchem-1477	41	21	as	as	ADP
eurjchem-1477	41	22	eluent	eluent	NOUN
eurjchem-1477	41	23	with	with	ADP
eurjchem-1477	41	24	iodine	iodine	NOUN
eurjchem-1477	41	25	as	as	ADP
eurjchem-1477	41	26	developing	develop	VERB
eurjchem-1477	41	27	agents	agent	NOUN
eurjchem-1477	41	28	.	.	PUNCT
eurjchem-1477	42	1	melting	melt	VERB
eurjchem-1477	42	2	points	point	NOUN
eurjchem-1477	42	3	of	of	ADP
eurjchem-1477	42	4	the	the	DET
eurjchem-1477	42	5	synthesised	synthesise	VERB
eurjchem-1477	42	6	compounds	compound	NOUN
eurjchem-1477	42	7	were	be	AUX
eurjchem-1477	42	8	recorded	record	VERB
eurjchem-1477	42	9	on	on	ADP
eurjchem-1477	42	10	open	open	ADJ
eurjchem-1477	42	11	capillaries	capillary	NOUN
eurjchem-1477	42	12	and	and	CCONJ
eurjchem-1477	42	13	are	be	AUX
eurjchem-1477	42	14	uncorrected	uncorrecte	VERB
eurjchem-1477	42	15	.	.	PUNCT
eurjchem-1477	43	1	1h	1h	NUM
eurjchem-1477	43	2	nmr	nmr	NOUN
eurjchem-1477	43	3	(	(	PUNCT
eurjchem-1477	43	4	400	400	NUM
eurjchem-1477	43	5	mhz	mhz	NOUN
eurjchem-1477	43	6	)	)	PUNCT
eurjchem-1477	43	7	and	and	CCONJ
eurjchem-1477	43	8	13c	13c	NOUN
eurjchem-1477	43	9	nmr	nmr	NOUN
eurjchem-1477	43	10	(	(	PUNCT
eurjchem-1477	43	11	100	100	NUM
eurjchem-1477	43	12	mhz	mhz	NOUN
eurjchem-1477	43	13	)	)	PUNCT
eurjchem-1477	43	14	spectra	spectra	NOUN
eurjchem-1477	43	15	were	be	AUX
eurjchem-1477	43	16	recorded	record	VERB
eurjchem-1477	43	17	on	on	ADP
eurjchem-1477	43	18	bruker	bruker	NOUN
eurjchem-1477	43	19	and	and	CCONJ
eurjchem-1477	43	20	varian	varian	PROPN
eurjchem-1477	43	21	spectrometer	spectrometer	NOUN
eurjchem-1477	43	22	using	use	VERB
eurjchem-1477	43	23	cdcl3	cdcl3	NOUN
eurjchem-1477	43	24	as	as	ADP
eurjchem-1477	43	25	solvent	solvent	NOUN
eurjchem-1477	43	26	and	and	CCONJ
eurjchem-1477	43	27	tms	tms	PROPN
eurjchem-1477	43	28	as	as	ADP
eurjchem-1477	43	29	internal	internal	ADJ
eurjchem-1477	43	30	standard	standard	NOUN
eurjchem-1477	43	31	.	.	PUNCT
eurjchem-1477	44	1	mass	mass	PROPN
eurjchem-1477	44	2	spectra	spectra	PROPN
eurjchem-1477	44	3	were	be	AUX
eurjchem-1477	44	4	recorded	record	VERB
eurjchem-1477	44	5	on	on	ADP
eurjchem-1477	44	6	agilent	agilent	PROPN
eurjchem-1477	44	7	6330	6330	NUM
eurjchem-1477	44	8	instrument	instrument	NOUN
eurjchem-1477	44	9	.	.	PUNCT
eurjchem-1477	45	1	elemental	elemental	ADJ
eurjchem-1477	45	2	analysis	analysis	NOUN
eurjchem-1477	45	3	was	be	AUX
eurjchem-1477	45	4	performed	perform	VERB
eurjchem-1477	45	5	using	use	VERB
eurjchem-1477	45	6	elemental	elemental	ADJ
eurjchem-1477	45	7	analysis	analysis	NOUN
eurjchem-1477	45	8	perkin‐elmer	perkin‐elmer	NOUN
eurjchem-1477	45	9	2400	2400	NUM
eurjchem-1477	45	10	.	.	PUNCT
eurjchem-1477	46	1	2.2	2.2	NUM
eurjchem-1477	46	2	.	.	PUNCT
eurjchem-1477	46	3	synthesis	synthesis	NOUN
eurjchem-1477	46	4	2.2.1	2.2.1	NUM
eurjchem-1477	46	5	.	.	PUNCT
eurjchem-1477	46	6	general	general	ADJ
eurjchem-1477	46	7	procedure	procedure	NOUN
eurjchem-1477	46	8	for	for	ADP
eurjchem-1477	46	9	the	the	DET
eurjchem-1477	46	10	synthesis	synthesis	NOUN
eurjchem-1477	46	11	of	of	ADP
eurjchem-1477	46	12	substituted	substitute	VERB
eurjchem-1477	46	13	phenyl	phenyl	NOUN
eurjchem-1477	46	14	acetamide	acetamide	NOUN
eurjchem-1477	46	15	analogues	analogue	NOUN
eurjchem-1477	46	16	(	(	PUNCT
eurjchem-1477	46	17	2a‐k	2a‐k	NOUN
eurjchem-1477	46	18	)	)	PUNCT
eurjchem-1477	46	19	substituted	substitute	VERB
eurjchem-1477	46	20	phenyl	phenyl	NOUN
eurjchem-1477	46	21	acetic	acetic	ADJ
eurjchem-1477	46	22	acids	acid	NOUN
eurjchem-1477	46	23	(	(	PUNCT
eurjchem-1477	46	24	0.6	0.6	NUM
eurjchem-1477	46	25	mmol	mmol	NOUN
eurjchem-1477	46	26	)	)	PUNCT
eurjchem-1477	46	27	,	,	PUNCT
eurjchem-1477	46	28	triethylamine	triethylamine	NOUN
eurjchem-1477	46	29	(	(	PUNCT
eurjchem-1477	46	30	1.6	1.6	NUM
eurjchem-1477	46	31	ml	ml	NOUN
eurjchem-1477	46	32	,	,	PUNCT
eurjchem-1477	46	33	1.2	1.2	NUM
eurjchem-1477	46	34	mmol	mmol	NOUN
eurjchem-1477	46	35	)	)	PUNCT
eurjchem-1477	46	36	and	and	CCONJ
eurjchem-1477	46	37	(	(	PUNCT
eurjchem-1477	46	38	2‐(1h‐benzotriazol‐1‐yl)‐1,1,3,3‐	2‐(1h‐benzotriazol‐1‐yl)‐1,1,3,3‐	NUM
eurjchem-1477	46	39	tetramethyluronium	tetramethyluronium	NOUN
eurjchem-1477	46	40	hexafluorophosphate	hexafluorophosphate	NOUN
eurjchem-1477	46	41	(	(	PUNCT
eurjchem-1477	46	42	hbtu	hbtu	NOUN
eurjchem-1477	46	43	)	)	PUNCT
eurjchem-1477	46	44	(	(	PUNCT
eurjchem-1477	46	45	2.2	2.2	NUM
eurjchem-1477	46	46	g	g	NOUN
eurjchem-1477	46	47	,	,	PUNCT
eurjchem-1477	46	48	0.6	0.6	NUM
eurjchem-1477	46	49	mmol	mmol	NOUN
eurjchem-1477	46	50	)	)	PUNCT
eurjchem-1477	46	51	were	be	AUX
eurjchem-1477	46	52	stirred	stir	VERB
eurjchem-1477	46	53	in	in	ADP
eurjchem-1477	46	54	5	5	NUM
eurjchem-1477	46	55	ml	ml	NOUN
eurjchem-1477	46	56	of	of	ADP
eurjchem-1477	46	57	dry	dry	ADJ
eurjchem-1477	46	58	dmf	dmf	PROPN
eurjchem-1477	46	59	for	for	ADP
eurjchem-1477	46	60	about	about	ADV
eurjchem-1477	46	61	10	10	NUM
eurjchem-1477	46	62	min	min	NOUN
eurjchem-1477	46	63	at	at	ADP
eurjchem-1477	46	64	room	room	NOUN
eurjchem-1477	46	65	temperature	temperature	NOUN
eurjchem-1477	46	66	.	.	PUNCT
eurjchem-1477	47	1	to	to	ADP
eurjchem-1477	47	2	that	that	DET
eurjchem-1477	47	3	reaction	reaction	NOUN
eurjchem-1477	47	4	mixture	mixture	NOUN
eurjchem-1477	47	5	amino	amino	NOUN
eurjchem-1477	47	6	acetal‐	acetal‐	PUNCT
eurjchem-1477	47	7	dehyde	dehyde	PROPN
eurjchem-1477	47	8	dimethyl	dimethyl	NOUN
eurjchem-1477	47	9	acetal	acetal	NOUN
eurjchem-1477	47	10	(	(	PUNCT
eurjchem-1477	47	11	0.78	0.78	NUM
eurjchem-1477	47	12	ml	ml	NOUN
eurjchem-1477	47	13	,	,	PUNCT
eurjchem-1477	47	14	0.7	0.7	NUM
eurjchem-1477	47	15	mmol	mmol	NOUN
eurjchem-1477	47	16	)	)	PUNCT
eurjchem-1477	47	17	was	be	AUX
eurjchem-1477	47	18	added	add	VERB
eurjchem-1477	47	19	slowly	slowly	ADV
eurjchem-1477	47	20	and	and	CCONJ
eurjchem-1477	47	21	stirring	stirring	NOUN
eurjchem-1477	47	22	was	be	AUX
eurjchem-1477	47	23	continued	continue	VERB
eurjchem-1477	47	24	for	for	ADP
eurjchem-1477	47	25	about	about	ADP
eurjchem-1477	47	26	4‐5	4‐5	NUM
eurjchem-1477	47	27	hrs	hrs	NOUN
eurjchem-1477	47	28	at	at	ADP
eurjchem-1477	47	29	room	room	NOUN
eurjchem-1477	47	30	temperature	temperature	NOUN
eurjchem-1477	47	31	.	.	PUNCT
eurjchem-1477	48	1	after	after	ADP
eurjchem-1477	48	2	the	the	DET
eurjchem-1477	48	3	completion	completion	NOUN
eurjchem-1477	48	4	of	of	ADP
eurjchem-1477	48	5	reaction	reaction	NOUN
eurjchem-1477	48	6	as	as	SCONJ
eurjchem-1477	48	7	indicated	indicate	VERB
eurjchem-1477	48	8	by	by	ADP
eurjchem-1477	48	9	tlc	tlc	NOUN
eurjchem-1477	48	10	,	,	PUNCT
eurjchem-1477	48	11	reaction	reaction	NOUN
eurjchem-1477	48	12	mixture	mixture	NOUN
eurjchem-1477	48	13	was	be	AUX
eurjchem-1477	48	14	quenched	quench	VERB
eurjchem-1477	48	15	with	with	ADP
eurjchem-1477	48	16	water	water	NOUN
eurjchem-1477	48	17	(	(	PUNCT
eurjchem-1477	48	18	40	40	NUM
eurjchem-1477	48	19	ml	ml	NOUN
eurjchem-1477	48	20	)	)	PUNCT
eurjchem-1477	48	21	and	and	CCONJ
eurjchem-1477	48	22	extracted	extract	VERB
eurjchem-1477	48	23	with	with	ADP
eurjchem-1477	48	24	ethyl	ethyl	PROPN
eurjchem-1477	48	25	acetate	acetate	NOUN
eurjchem-1477	48	26	.	.	PUNCT
eurjchem-1477	49	1	combined	combine	VERB
eurjchem-1477	49	2	ethyl	ethyl	PROPN
eurjchem-1477	49	3	acetate	acetate	NOUN
eurjchem-1477	49	4	layer	layer	NOUN
eurjchem-1477	49	5	was	be	AUX
eurjchem-1477	49	6	washed	wash	VERB
eurjchem-1477	49	7	with	with	ADP
eurjchem-1477	49	8	saturated	saturate	VERB
eurjchem-1477	49	9	sodium	sodium	NOUN
eurjchem-1477	49	10	bicarbonate	bicarbonate	NOUN
eurjchem-1477	49	11	solution	solution	NOUN
eurjchem-1477	49	12	(	(	PUNCT
eurjchem-1477	49	13	20	20	NUM
eurjchem-1477	49	14	ml	ml	NOUN
eurjchem-1477	49	15	×	×	NOUN
eurjchem-1477	49	16	2	2	NUM
eurjchem-1477	49	17	)	)	PUNCT
eurjchem-1477	49	18	,	,	PUNCT
eurjchem-1477	49	19	followed	follow	VERB
eurjchem-1477	49	20	by	by	ADP
eurjchem-1477	49	21	brine	brine	NOUN
eurjchem-1477	49	22	solution	solution	NOUN
eurjchem-1477	49	23	and	and	CCONJ
eurjchem-1477	49	24	water	water	NOUN
eurjchem-1477	49	25	(	(	PUNCT
eurjchem-1477	49	26	20	20	NUM
eurjchem-1477	49	27	ml	ml	NOUN
eurjchem-1477	49	28	×	×	NOUN
eurjchem-1477	49	29	3	3	NUM
eurjchem-1477	49	30	)	)	PUNCT
eurjchem-1477	49	31	,	,	PUNCT
eurjchem-1477	49	32	dried	dry	VERB
eurjchem-1477	49	33	over	over	ADP
eurjchem-1477	49	34	anhydrous	anhydrous	ADJ
eurjchem-1477	49	35	sodium	sodium	NOUN
eurjchem-1477	49	36	sulphate	sulphate	NOUN
eurjchem-1477	49	37	.	.	PUNCT
eurjchem-1477	50	1	solvent	solvent	PROPN
eurjchem-1477	50	2	was	be	AUX
eurjchem-1477	50	3	removed	remove	VERB
eurjchem-1477	50	4	under	under	ADP
eurjchem-1477	50	5	reduced	reduce	VERB
eurjchem-1477	50	6	pressure	pressure	NOUN
eurjchem-1477	50	7	and	and	CCONJ
eurjchem-1477	50	8	obtained	obtain	VERB
eurjchem-1477	50	9	crude	crude	ADJ
eurjchem-1477	50	10	product	product	NOUN
eurjchem-1477	50	11	was	be	AUX
eurjchem-1477	50	12	recrystal‐	recrystal‐	NUM
eurjchem-1477	50	13	lized	lize	VERB
eurjchem-1477	50	14	using	use	VERB
eurjchem-1477	50	15	petroleum	petroleum	NOUN
eurjchem-1477	50	16	ether	ether	NOUN
eurjchem-1477	50	17	(	(	PUNCT
eurjchem-1477	50	18	scheme	scheme	NOUN
eurjchem-1477	50	19	1	1	NUM
eurjchem-1477	50	20	)	)	PUNCT
eurjchem-1477	50	21	.	.	PUNCT
eurjchem-1477	51	1	2.2.2	2.2.2	X
eurjchem-1477	51	2	.	.	PUNCT
eurjchem-1477	51	3	general	general	ADJ
eurjchem-1477	51	4	procedure	procedure	NOUN
eurjchem-1477	51	5	for	for	ADP
eurjchem-1477	51	6	the	the	DET
eurjchem-1477	51	7	synthesis	synthesis	NOUN
eurjchem-1477	51	8	of	of	ADP
eurjchem-1477	51	9	3‐benzazepi‐	3‐benzazepi‐	NUM
eurjchem-1477	51	10	nones	none	NOUN
eurjchem-1477	51	11	(	(	PUNCT
eurjchem-1477	51	12	3a‐k	3a‐k	ADJ
eurjchem-1477	51	13	)	)	PUNCT
eurjchem-1477	51	14	eaton	eaton	PROPN
eurjchem-1477	51	15	’s	’s	PART
eurjchem-1477	51	16	reagent	reagent	NOUN
eurjchem-1477	51	17	(	(	PUNCT
eurjchem-1477	51	18	1.5	1.5	NUM
eurjchem-1477	51	19	mmol	mmol	NOUN
eurjchem-1477	51	20	)	)	PUNCT
eurjchem-1477	51	21	was	be	AUX
eurjchem-1477	51	22	slowly	slowly	ADV
eurjchem-1477	51	23	added	add	VERB
eurjchem-1477	51	24	to	to	ADP
eurjchem-1477	51	25	substituted	substitute	VERB
eurjchem-1477	51	26	phenyl	phenyl	NOUN
eurjchem-1477	51	27	acetamide	acetamide	NOUN
eurjchem-1477	51	28	analogues	analogue	NOUN
eurjchem-1477	51	29	(	(	PUNCT
eurjchem-1477	51	30	1	1	NUM
eurjchem-1477	51	31	g	g	NOUN
eurjchem-1477	51	32	,	,	PUNCT
eurjchem-1477	51	33	0.39	0.39	NUM
eurjchem-1477	51	34	mmol	mmol	NOUN
eurjchem-1477	51	35	)	)	PUNCT
eurjchem-1477	51	36	and	and	CCONJ
eurjchem-1477	51	37	stirred	stir	VERB
eurjchem-1477	51	38	at	at	ADP
eurjchem-1477	51	39	room	room	NOUN
eurjchem-1477	51	40	temperature	temperature	NOUN
eurjchem-1477	51	41	for	for	ADP
eurjchem-1477	51	42	about	about	ADV
eurjchem-1477	51	43	10‐15	10‐15	NUM
eurjchem-1477	51	44	min	min	PROPN
eurjchem-1477	51	45	.	.	PROPN
eurjchem-1477	51	46	completion	completion	NOUN
eurjchem-1477	51	47	of	of	ADP
eurjchem-1477	51	48	reaction	reaction	NOUN
eurjchem-1477	51	49	was	be	AUX
eurjchem-1477	51	50	monitored	monitor	VERB
eurjchem-1477	51	51	by	by	ADP
eurjchem-1477	51	52	tlc	tlc	PROPN
eurjchem-1477	51	53	.	.	PUNCT
eurjchem-1477	52	1	after	after	ADP
eurjchem-1477	52	2	the	the	DET
eurjchem-1477	52	3	completion	completion	NOUN
eurjchem-1477	52	4	of	of	ADP
eurjchem-1477	52	5	reaction	reaction	NOUN
eurjchem-1477	52	6	,	,	PUNCT
eurjchem-1477	52	7	reaction	reaction	NOUN
eurjchem-1477	52	8	mixture	mixture	NOUN
eurjchem-1477	52	9	was	be	AUX
eurjchem-1477	52	10	slowly	slowly	ADV
eurjchem-1477	52	11	added	add	VERB
eurjchem-1477	52	12	to	to	ADP
eurjchem-1477	52	13	cold	cold	ADJ
eurjchem-1477	52	14	saturated	saturate	VERB
eurjchem-1477	52	15	solution	solution	NOUN
eurjchem-1477	52	16	of	of	ADP
eurjchem-1477	52	17	sodium	sodium	NOUN
eurjchem-1477	52	18	bicarbonate	bicarbonate	NOUN
eurjchem-1477	52	19	and	and	CCONJ
eurjchem-1477	52	20	precipitated	precipitate	VERB
eurjchem-1477	52	21	gummy	gummy	ADJ
eurjchem-1477	52	22	residue	residue	NOUN
eurjchem-1477	52	23	was	be	AUX
eurjchem-1477	52	24	recrystallized	recrystallize	VERB
eurjchem-1477	52	25	from	from	ADP
eurjchem-1477	52	26	n‐hexane	n‐hexane	X
eurjchem-1477	52	27	(	(	PUNCT
eurjchem-1477	52	28	scheme	scheme	NOUN
eurjchem-1477	52	29	1	1	NUM
eurjchem-1477	52	30	)	)	PUNCT
eurjchem-1477	52	31	.	.	PUNCT
eurjchem-1477	53	1	8‐methoxy‐1,3‐dihydro	8‐methoxy‐1,3‐dihydro	NUM
eurjchem-1477	53	2	benzo[d]azepin‐2‐one	benzo[d]azepin‐2‐one	NUM
eurjchem-1477	53	3	(	(	PUNCT
eurjchem-1477	53	4	3a	3a	NUM
eurjchem-1477	53	5	):	):	PUNCT
eurjchem-1477	53	6	color	color	NOUN
eurjchem-1477	53	7	:	:	PUNCT
eurjchem-1477	53	8	pale	pale	ADJ
eurjchem-1477	53	9	yellow	yellow	ADJ
eurjchem-1477	53	10	solid	solid	ADJ
eurjchem-1477	53	11	.	.	PUNCT
eurjchem-1477	53	12	yield	yield	NOUN
eurjchem-1477	53	13	:	:	PUNCT
eurjchem-1477	53	14	90	90	NUM
eurjchem-1477	53	15	%	%	NOUN
eurjchem-1477	53	16	.	.	PUNCT
eurjchem-1477	54	1	m.p	m.p	PROPN
eurjchem-1477	54	2	.	.	PROPN
eurjchem-1477	54	3	:	:	PUNCT
eurjchem-1477	54	4	158‐159	158‐159	PROPN
eurjchem-1477	54	5	°	°	PROPN
eurjchem-1477	54	6	c	c	PROPN
eurjchem-1477	54	7	.	.	PUNCT
eurjchem-1477	55	1	1h	1h	NUM
eurjchem-1477	55	2	nmr	nmr	NOUN
eurjchem-1477	55	3	(	(	PUNCT
eurjchem-1477	55	4	400	400	NUM
eurjchem-1477	55	5	mhz	mhz	NOUN
eurjchem-1477	55	6	,	,	PUNCT
eurjchem-1477	55	7	cdcl3	cdcl3	PROPN
eurjchem-1477	55	8	,	,	PUNCT
eurjchem-1477	55	9	δ	δ	PROPN
eurjchem-1477	55	10	,	,	PUNCT
eurjchem-1477	55	11	ppm	ppm	NUM
eurjchem-1477	55	12	):	):	PUNCT
eurjchem-1477	55	13	3.48	3.48	NUM
eurjchem-1477	55	14	(	(	PUNCT
eurjchem-1477	55	15	s	s	PROPN
eurjchem-1477	55	16	,	,	PUNCT
eurjchem-1477	55	17	2h	2h	NUM
eurjchem-1477	55	18	,	,	PUNCT
eurjchem-1477	55	19	azepine‐ch2	azepine‐ch2	NUM
eurjchem-1477	55	20	)	)	PUNCT
eurjchem-1477	55	21	,	,	PUNCT
eurjchem-1477	55	22	3.81	3.81	NUM
eurjchem-1477	55	23	(	(	PUNCT
eurjchem-1477	55	24	s	s	PROPN
eurjchem-1477	55	25	,	,	PUNCT
eurjchem-1477	55	26	3h	3h	NUM
eurjchem-1477	55	27	,	,	PUNCT
eurjchem-1477	55	28	och3	och3	ADJ
eurjchem-1477	55	29	)	)	PUNCT
eurjchem-1477	55	30	,	,	PUNCT
eurjchem-1477	55	31	6.18‐6.17	6.18‐6.17	PROPN
eurjchem-1477	55	32	(	(	PUNCT
eurjchem-1477	55	33	d	d	PROPN
eurjchem-1477	55	34	,	,	PUNCT
eurjchem-1477	55	35	1h	1h	NUM
eurjchem-1477	55	36	,	,	PUNCT
eurjchem-1477	55	37	j	j	PROPN
eurjchem-1477	55	38	=	=	SYM
eurjchem-1477	55	39	4.0	4.0	NUM
eurjchem-1477	55	40	hz	hz	NOUN
eurjchem-1477	55	41	,	,	PUNCT
eurjchem-1477	55	42	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	55	43	)	)	PUNCT
eurjchem-1477	55	44	,	,	PUNCT
eurjchem-1477	55	45	6.34‐6.31	6.34‐6.31	NUM
eurjchem-1477	55	46	(	(	PUNCT
eurjchem-1477	55	47	d	d	NOUN
eurjchem-1477	55	48	,	,	PUNCT
eurjchem-1477	55	49	1h	1h	NUM
eurjchem-1477	55	50	,	,	PUNCT
eurjchem-1477	55	51	j	j	PROPN
eurjchem-1477	55	52	=	=	SYM
eurjchem-1477	55	53	9.2	9.2	NUM
eurjchem-1477	55	54	hz	hz	VERB
eurjchem-1477	55	55	,	,	PUNCT
eurjchem-1477	55	56	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	55	57	)	)	PUNCT
eurjchem-1477	55	58	,	,	PUNCT
eurjchem-1477	55	59	6.80	6.80	NUM
eurjchem-1477	55	60	(	(	PUNCT
eurjchem-1477	55	61	s	s	PROPN
eurjchem-1477	55	62	,	,	PUNCT
eurjchem-1477	55	63	1h	1h	NUM
eurjchem-1477	55	64	,	,	PUNCT
eurjchem-1477	55	65	ar‐h	ar‐h	NOUN
eurjchem-1477	55	66	)	)	PUNCT
eurjchem-1477	55	67	,	,	PUNCT
eurjchem-1477	55	68	6.87‐6.86	6.87‐6.86	PROPN
eurjchem-1477	55	69	(	(	PUNCT
eurjchem-1477	55	70	d	d	PROPN
eurjchem-1477	55	71	,	,	PUNCT
eurjchem-1477	55	72	1h	1h	NUM
eurjchem-1477	55	73	,	,	PUNCT
eurjchem-1477	55	74	j	j	PROPN
eurjchem-1477	55	75	=	=	SYM
eurjchem-1477	55	76	2.4	2.4	NUM
eurjchem-1477	55	77	hz	hz	NOUN
eurjchem-1477	55	78	,	,	PUNCT
eurjchem-1477	55	79	ar‐h	ar‐h	PROPN
eurjchem-1477	55	80	)	)	PUNCT
eurjchem-1477	55	81	,	,	PUNCT
eurjchem-1477	55	82	7.17‐7.15	7.17‐7.15	PROPN
eurjchem-1477	55	83	(	(	PUNCT
eurjchem-1477	55	84	d	d	PROPN
eurjchem-1477	55	85	,	,	PUNCT
eurjchem-1477	55	86	1h	1h	NUM
eurjchem-1477	55	87	,	,	PUNCT
eurjchem-1477	55	88	j	j	PROPN
eurjchem-1477	56	1	=	=	PROPN
eurjchem-1477	56	2	8.4	8.4	NUM
eurjchem-1477	56	3	hz	hz	NOUN
eurjchem-1477	56	4	,	,	PUNCT
eurjchem-1477	56	5	ar‐h	ar‐h	PROPN
eurjchem-1477	56	6	)	)	PUNCT
eurjchem-1477	56	7	,	,	PUNCT
eurjchem-1477	56	8	8.44	8.44	NUM
eurjchem-1477	56	9	(	(	PUNCT
eurjchem-1477	56	10	s	s	PROPN
eurjchem-1477	56	11	,	,	PUNCT
eurjchem-1477	56	12	1h	1h	NUM
eurjchem-1477	56	13	,	,	PUNCT
eurjchem-1477	56	14	nh	nh	PROPN
eurjchem-1477	56	15	)	)	PUNCT
eurjchem-1477	56	16	.	.	PUNCT
eurjchem-1477	57	1	13c	13c	NOUN
eurjchem-1477	57	2	nmr	nmr	NOUN
eurjchem-1477	57	3	(	(	PUNCT
eurjchem-1477	57	4	100	100	NUM
eurjchem-1477	57	5	mhz	mhz	NOUN
eurjchem-1477	57	6	,	,	PUNCT
eurjchem-1477	57	7	cdcl3	cdcl3	PROPN
eurjchem-1477	57	8	,	,	PUNCT
eurjchem-1477	57	9	δ	δ	PROPN
eurjchem-1477	57	10	,	,	PUNCT
eurjchem-1477	57	11	ppm	ppm	NUM
eurjchem-1477	57	12	):	):	PUNCT
eurjchem-1477	57	13	170.40	170.40	NUM
eurjchem-1477	57	14	(	(	PUNCT
eurjchem-1477	57	15	1c	1c	NOUN
eurjchem-1477	57	16	,	,	PUNCT
eurjchem-1477	57	17	conh	conh	NOUN
eurjchem-1477	57	18	)	)	PUNCT
eurjchem-1477	57	19	,	,	PUNCT
eurjchem-1477	57	20	160.44	160.44	NUM
eurjchem-1477	57	21	(	(	PUNCT
eurjchem-1477	57	22	1c	1c	NOUN
eurjchem-1477	57	23	,	,	PUNCT
eurjchem-1477	57	24	ar‐c	ar‐c	PROPN
eurjchem-1477	57	25	)	)	PUNCT
eurjchem-1477	57	26	,	,	PUNCT
eurjchem-1477	57	27	132.52	132.52	NUM
eurjchem-1477	57	28	(	(	PUNCT
eurjchem-1477	57	29	1c	1c	NUM
eurjchem-1477	57	30	,	,	PUNCT
eurjchem-1477	57	31	ar‐c	ar‐c	PROPN
eurjchem-1477	57	32	)	)	PUNCT
eurjchem-1477	57	33	,	,	PUNCT
eurjchem-1477	57	34	128.8	128.8	NUM
eurjchem-1477	57	35	(	(	PUNCT
eurjchem-1477	57	36	1c	1c	NUM
eurjchem-1477	57	37	,	,	PUNCT
eurjchem-1477	57	38	ar‐c	ar‐c	PROPN
eurjchem-1477	57	39	)	)	PUNCT
eurjchem-1477	57	40	,	,	PUNCT
eurjchem-1477	57	41	127.22	127.22	NUM
eurjchem-1477	57	42	(	(	PUNCT
eurjchem-1477	57	43	1c	1c	NUM
eurjchem-1477	57	44	,	,	PUNCT
eurjchem-1477	57	45	ar‐c	ar‐c	PROPN
eurjchem-1477	57	46	)	)	PUNCT
eurjchem-1477	57	47	,	,	PUNCT
eurjchem-1477	57	48	122.70	122.70	NUM
eurjchem-1477	57	49	(	(	PUNCT
eurjchem-1477	57	50	1c	1c	NUM
eurjchem-1477	57	51	,	,	PUNCT
eurjchem-1477	57	52	ch‐nh	ch‐nh	NOUN
eurjchem-1477	57	53	)	)	PUNCT
eurjchem-1477	57	54	,	,	PUNCT
eurjchem-1477	57	55	116.63	116.63	NUM
eurjchem-1477	57	56	(	(	PUNCT
eurjchem-1477	57	57	1c	1c	NOUN
eurjchem-1477	57	58	,	,	PUNCT
eurjchem-1477	57	59	ar‐c	ar‐c	PROPN
eurjchem-1477	57	60	)	)	PUNCT
eurjchem-1477	57	61	,	,	PUNCT
eurjchem-1477	57	62	113.88	113.88	NUM
eurjchem-1477	57	63	(	(	PUNCT
eurjchem-1477	57	64	1c	1c	NUM
eurjchem-1477	57	65	,	,	PUNCT
eurjchem-1477	57	66	ar‐c	ar‐c	PROPN
eurjchem-1477	57	67	)	)	PUNCT
eurjchem-1477	57	68	,	,	PUNCT
eurjchem-1477	57	69	113.35	113.35	NUM
eurjchem-1477	57	70	(	(	PUNCT
eurjchem-1477	57	71	1c	1c	NOUN
eurjchem-1477	57	72	,	,	PUNCT
eurjchem-1477	57	73	ch‐chnh	ch‐chnh	PROPN
eurjchem-1477	57	74	)	)	PUNCT
eurjchem-1477	57	75	,	,	PUNCT
eurjchem-1477	57	76	55.50	55.50	NUM
eurjchem-1477	57	77	(	(	PUNCT
eurjchem-1477	57	78	1c	1c	NOUN
eurjchem-1477	57	79	,	,	PUNCT
eurjchem-1477	57	80	och3	och3	ADJ
eurjchem-1477	57	81	)	)	PUNCT
eurjchem-1477	57	82	,	,	PUNCT
eurjchem-1477	57	83	43.66	43.66	NUM
eurjchem-1477	57	84	(	(	PUNCT
eurjchem-1477	57	85	1c	1c	NOUN
eurjchem-1477	57	86	,	,	PUNCT
eurjchem-1477	57	87	ch2‐conh	ch2‐conh	NOUN
eurjchem-1477	57	88	)	)	PUNCT
eurjchem-1477	57	89	.	.	PUNCT
eurjchem-1477	58	1	ms	ms	NOUN
eurjchem-1477	58	2	(	(	PUNCT
eurjchem-1477	58	3	ei	ei	PROPN
eurjchem-1477	58	4	,	,	PUNCT
eurjchem-1477	58	5	m	m	PROPN
eurjchem-1477	58	6	/	/	SYM
eurjchem-1477	58	7	z	z	NOUN
eurjchem-1477	58	8	):	):	PUNCT
eurjchem-1477	58	9	190.2111	190.2111	NUM
eurjchem-1477	58	10	(	(	PUNCT
eurjchem-1477	58	11	m+1	m+1	NUM
eurjchem-1477	58	12	)	)	PUNCT
eurjchem-1477	58	13	.	.	PUNCT
eurjchem-1477	59	1	anal	anal	PROPN
eurjchem-1477	59	2	.	.	PUNCT
eurjchem-1477	59	3	calcd	calcd	NOUN
eurjchem-1477	59	4	.	.	PUNCT
eurjchem-1477	60	1	for	for	ADP
eurjchem-1477	60	2	c11h11no2	c11h11no2	PROPN
eurjchem-1477	60	3	:	:	PUNCT
eurjchem-1477	60	4	c	c	X
eurjchem-1477	60	5	,	,	PUNCT
eurjchem-1477	60	6	69.83	69.83	NUM
eurjchem-1477	60	7	;	;	PUNCT
eurjchem-1477	60	8	h	h	NOUN
eurjchem-1477	60	9	,	,	PUNCT
eurjchem-1477	60	10	5.86	5.86	NUM
eurjchem-1477	60	11	;	;	PUNCT
eurjchem-1477	60	12	n	n	CCONJ
eurjchem-1477	60	13	,	,	PUNCT
eurjchem-1477	60	14	7.40	7.40	NUM
eurjchem-1477	60	15	;	;	PUNCT
eurjchem-1477	60	16	o	o	NOUN
eurjchem-1477	60	17	,	,	PUNCT
eurjchem-1477	60	18	16.91	16.91	NUM
eurjchem-1477	60	19	.	.	PUNCT
eurjchem-1477	60	20	found	find	VERB
eurjchem-1477	60	21	:	:	PUNCT
eurjchem-1477	61	1	c	c	X
eurjchem-1477	61	2	,	,	PUNCT
eurjchem-1477	61	3	69.86	69.86	NUM
eurjchem-1477	61	4	;	;	PUNCT
eurjchem-1477	61	5	h	h	NOUN
eurjchem-1477	61	6	,	,	PUNCT
eurjchem-1477	61	7	5.84	5.84	NUM
eurjchem-1477	61	8	;	;	PUNCT
eurjchem-1477	61	9	n	n	CCONJ
eurjchem-1477	61	10	,	,	PUNCT
eurjchem-1477	61	11	7.44	7.44	NUM
eurjchem-1477	61	12	;	;	PUNCT
eurjchem-1477	61	13	o	o	NOUN
eurjchem-1477	61	14	,	,	PUNCT
eurjchem-1477	61	15	16.89	16.89	NUM
eurjchem-1477	61	16	%	%	NOUN
eurjchem-1477	61	17	.	.	PUNCT
eurjchem-1477	62	1	7‐methyl‐1	7‐methyl‐1	NUM
eurjchem-1477	62	2	,	,	PUNCT
eurjchem-1477	62	3	3‐dihydro‐benzo[d]azepin‐2‐one	3‐dihydro‐benzo[d]azepin‐2‐one	NUM
eurjchem-1477	62	4	(	(	PUNCT
eurjchem-1477	62	5	3b	3b	NUM
eurjchem-1477	62	6	):	):	PUNCT
eurjchem-1477	62	7	color	color	NOUN
eurjchem-1477	62	8	:	:	PUNCT
eurjchem-1477	62	9	dark	dark	ADJ
eurjchem-1477	62	10	brown	brown	PROPN
eurjchem-1477	62	11	semi	semi	X
eurjchem-1477	62	12	solid	solid	ADJ
eurjchem-1477	62	13	.	.	PUNCT
eurjchem-1477	62	14	yield	yield	NOUN
eurjchem-1477	62	15	:	:	PUNCT
eurjchem-1477	62	16	89	89	NUM
eurjchem-1477	62	17	%	%	NOUN
eurjchem-1477	62	18	.	.	PUNCT
eurjchem-1477	63	1	m.p	m.p	PROPN
eurjchem-1477	63	2	.	.	PROPN
eurjchem-1477	63	3	:	:	PUNCT
eurjchem-1477	64	1	116‐118	116‐118	NUM
eurjchem-1477	64	2	°	°	PROPN
eurjchem-1477	64	3	c	c	PROPN
eurjchem-1477	64	4	.	.	PUNCT
eurjchem-1477	65	1	1h	1h	NUM
eurjchem-1477	65	2	nmr	nmr	NOUN
eurjchem-1477	65	3	(	(	PUNCT
eurjchem-1477	65	4	400	400	NUM
eurjchem-1477	65	5	mhz	mhz	NOUN
eurjchem-1477	65	6	,	,	PUNCT
eurjchem-1477	65	7	cdcl3	cdcl3	PROPN
eurjchem-1477	65	8	,	,	PUNCT
eurjchem-1477	65	9	δ	δ	PROPN
eurjchem-1477	65	10	,	,	PUNCT
eurjchem-1477	65	11	ppm	ppm	NUM
eurjchem-1477	65	12	):	):	PUNCT
eurjchem-1477	65	13	2.38	2.38	NUM
eurjchem-1477	65	14	(	(	PUNCT
eurjchem-1477	65	15	s	s	PROPN
eurjchem-1477	65	16	,	,	PUNCT
eurjchem-1477	65	17	3h	3h	NUM
eurjchem-1477	65	18	,	,	PUNCT
eurjchem-1477	65	19	ch3	ch3	PROPN
eurjchem-1477	65	20	)	)	PUNCT
eurjchem-1477	65	21	,	,	PUNCT
eurjchem-1477	65	22	3.48	3.48	NUM
eurjchem-1477	65	23	(	(	PUNCT
eurjchem-1477	65	24	s	s	PROPN
eurjchem-1477	65	25	,	,	PUNCT
eurjchem-1477	65	26	2h	2h	NUM
eurjchem-1477	65	27	,	,	PUNCT
eurjchem-1477	65	28	azepine‐ch2	azepine‐ch2	NUM
eurjchem-1477	65	29	)	)	PUNCT
eurjchem-1477	65	30	,	,	PUNCT
eurjchem-1477	65	31	6.18‐6.17	6.18‐6.17	PROPN
eurjchem-1477	66	1	(	(	PUNCT
eurjchem-1477	66	2	d	d	PROPN
eurjchem-1477	66	3	,	,	PUNCT
eurjchem-1477	66	4	1h	1h	NUM
eurjchem-1477	66	5	,	,	PUNCT
eurjchem-1477	66	6	j	j	PROPN
eurjchem-1477	66	7	=	=	SYM
eurjchem-1477	66	8	4.4	4.4	NUM
eurjchem-1477	66	9	hz	hz	VERB
eurjchem-1477	66	10	,	,	PUNCT
eurjchem-1477	66	11	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	66	12	)	)	PUNCT
eurjchem-1477	66	13	,	,	PUNCT
eurjchem-1477	66	14	6.34‐	6.34‐	NUM
eurjchem-1477	66	15	6.31	6.31	NUM
eurjchem-1477	66	16	(	(	PUNCT
eurjchem-1477	66	17	d	d	PROPN
eurjchem-1477	66	18	,	,	PUNCT
eurjchem-1477	66	19	1h	1h	NUM
eurjchem-1477	66	20	,	,	PUNCT
eurjchem-1477	66	21	j	j	PROPN
eurjchem-1477	66	22	=	=	SYM
eurjchem-1477	66	23	9.1	9.1	NUM
eurjchem-1477	66	24	hz	hz	NOUN
eurjchem-1477	66	25	,	,	PUNCT
eurjchem-1477	66	26	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	66	27	)	)	PUNCT
eurjchem-1477	66	28	,	,	PUNCT
eurjchem-1477	66	29	6.95	6.95	NUM
eurjchem-1477	66	30	(	(	PUNCT
eurjchem-1477	66	31	s	s	PROPN
eurjchem-1477	66	32	,	,	PUNCT
eurjchem-1477	66	33	1h	1h	NUM
eurjchem-1477	66	34	,	,	PUNCT
eurjchem-1477	66	35	ar‐h	ar‐h	NOUN
eurjchem-1477	66	36	)	)	PUNCT
eurjchem-1477	66	37	,	,	PUNCT
eurjchem-1477	66	38	6.85‐	6.85‐	NUM
eurjchem-1477	66	39	6.84	6.84	NUM
eurjchem-1477	66	40	(	(	PUNCT
eurjchem-1477	66	41	d	d	PROPN
eurjchem-1477	66	42	,	,	PUNCT
eurjchem-1477	66	43	1h	1h	NUM
eurjchem-1477	66	44	,	,	PUNCT
eurjchem-1477	66	45	j	j	PROPN
eurjchem-1477	66	46	=	=	SYM
eurjchem-1477	66	47	7.2	7.2	NUM
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eurjchem-1477	66	49	,	,	PUNCT
eurjchem-1477	66	50	ar‐h	ar‐h	NOUN
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eurjchem-1477	66	52	,	,	PUNCT
eurjchem-1477	66	53	6.86‐6.87	6.86‐6.87	NUM
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eurjchem-1477	66	55	d	d	PROPN
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eurjchem-1477	66	57	1h	1h	NUM
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eurjchem-1477	66	60	=	=	SYM
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eurjchem-1477	66	62	hz	hz	NOUN
eurjchem-1477	66	63	,	,	PUNCT
eurjchem-1477	66	64	ar‐h	ar‐h	PROPN
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eurjchem-1477	66	66	,	,	PUNCT
eurjchem-1477	66	67	8.41	8.41	NUM
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eurjchem-1477	66	69	s	s	PROPN
eurjchem-1477	66	70	,	,	PUNCT
eurjchem-1477	66	71	1h	1h	NUM
eurjchem-1477	66	72	,	,	PUNCT
eurjchem-1477	66	73	nh	nh	PROPN
eurjchem-1477	66	74	)	)	PUNCT
eurjchem-1477	66	75	.	.	PUNCT
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eurjchem-1477	67	2	nmr	nmr	NOUN
eurjchem-1477	67	3	(	(	PUNCT
eurjchem-1477	67	4	100	100	NUM
eurjchem-1477	67	5	mhz	mhz	NOUN
eurjchem-1477	67	6	,	,	PUNCT
eurjchem-1477	67	7	cdcl3	cdcl3	PROPN
eurjchem-1477	67	8	,	,	PUNCT
eurjchem-1477	67	9	δ	δ	PROPN
eurjchem-1477	67	10	,	,	PUNCT
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eurjchem-1477	67	12	):	):	PUNCT
eurjchem-1477	67	13	169.40	169.40	NUM
eurjchem-1477	67	14	(	(	PUNCT
eurjchem-1477	67	15	1c	1c	X
eurjchem-1477	67	16	,	,	PUNCT
eurjchem-1477	67	17	conh	conh	NOUN
eurjchem-1477	67	18	)	)	PUNCT
eurjchem-1477	67	19	,	,	PUNCT
eurjchem-1477	67	20	160.44	160.44	NUM
eurjchem-1477	67	21	(	(	PUNCT
eurjchem-1477	67	22	1c	1c	NOUN
eurjchem-1477	67	23	,	,	PUNCT
eurjchem-1477	67	24	ar‐c	ar‐c	PROPN
eurjchem-1477	67	25	)	)	PUNCT
eurjchem-1477	67	26	,	,	PUNCT
eurjchem-1477	67	27	132.49	132.49	NUM
eurjchem-1477	67	28	(	(	PUNCT
eurjchem-1477	67	29	1c	1c	NOUN
eurjchem-1477	67	30	,	,	PUNCT
eurjchem-1477	67	31	ar‐c	ar‐c	PROPN
eurjchem-1477	67	32	)	)	PUNCT
eurjchem-1477	67	33	,	,	PUNCT
eurjchem-1477	67	34	128.51	128.51	NUM
eurjchem-1477	67	35	(	(	PUNCT
eurjchem-1477	67	36	1c	1c	NOUN
eurjchem-1477	67	37	,	,	PUNCT
eurjchem-1477	67	38	ar‐c	ar‐c	PROPN
eurjchem-1477	67	39	)	)	PUNCT
eurjchem-1477	67	40	,	,	PUNCT
eurjchem-1477	67	41	127.02	127.02	NUM
eurjchem-1477	67	42	(	(	PUNCT
eurjchem-1477	67	43	1c	1c	NOUN
eurjchem-1477	67	44	,	,	PUNCT
eurjchem-1477	67	45	ar‐c	ar‐c	PROPN
eurjchem-1477	67	46	)	)	PUNCT
eurjchem-1477	67	47	,	,	PUNCT
eurjchem-1477	67	48	122.50	122.50	NUM
eurjchem-1477	67	49	(	(	PUNCT
eurjchem-1477	67	50	1c	1c	NOUN
eurjchem-1477	67	51	,	,	PUNCT
eurjchem-1477	67	52	ar‐c	ar‐c	PROPN
eurjchem-1477	67	53	)	)	PUNCT
eurjchem-1477	67	54	,	,	PUNCT
eurjchem-1477	67	55	115.63	115.63	NUM
eurjchem-1477	67	56	(	(	PUNCT
eurjchem-1477	67	57	1c	1c	NOUN
eurjchem-1477	67	58	,	,	PUNCT
eurjchem-1477	67	59	ar‐c	ar‐c	PROPN
eurjchem-1477	67	60	)	)	PUNCT
eurjchem-1477	67	61	,	,	PUNCT
eurjchem-1477	67	62	113.66	113.66	NUM
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eurjchem-1477	67	64	1c	1c	NOUN
eurjchem-1477	67	65	,	,	PUNCT
eurjchem-1477	67	66	chnh	chnh	NOUN
eurjchem-1477	67	67	)	)	PUNCT
eurjchem-1477	67	68	,	,	PUNCT
eurjchem-1477	67	69	113.25	113.25	NUM
eurjchem-1477	67	70	(	(	PUNCT
eurjchem-1477	67	71	1c	1c	NOUN
eurjchem-1477	67	72	,	,	PUNCT
eurjchem-1477	67	73	ch‐chnh	ch‐chnh	PROPN
eurjchem-1477	67	74	)	)	PUNCT
eurjchem-1477	67	75	,	,	PUNCT
eurjchem-1477	67	76	56.23	56.23	NUM
eurjchem-1477	67	77	(	(	PUNCT
eurjchem-1477	67	78	1c	1c	NOUN
eurjchem-1477	67	79	,	,	PUNCT
eurjchem-1477	67	80	ch2‐	ch2‐	NOUN
eurjchem-1477	67	81	conh	conh	NOUN
eurjchem-1477	67	82	)	)	PUNCT
eurjchem-1477	67	83	,	,	PUNCT
eurjchem-1477	67	84	36.64	36.64	NUM
eurjchem-1477	67	85	(	(	PUNCT
eurjchem-1477	67	86	1c	1c	NOUN
eurjchem-1477	67	87	,	,	PUNCT
eurjchem-1477	67	88	ch3	ch3	PROPN
eurjchem-1477	67	89	)	)	PUNCT
eurjchem-1477	67	90	.	.	PUNCT
eurjchem-1477	68	1	ms	ms	PROPN
eurjchem-1477	68	2	(	(	PUNCT
eurjchem-1477	68	3	ei	ei	PROPN
eurjchem-1477	68	4	,	,	PUNCT
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eurjchem-1477	68	6	/	/	SYM
eurjchem-1477	68	7	z	z	NOUN
eurjchem-1477	68	8	):	):	PUNCT
eurjchem-1477	68	9	174.2174	174.2174	NUM
eurjchem-1477	68	10	(	(	PUNCT
eurjchem-1477	68	11	m+1	m+1	NUM
eurjchem-1477	68	12	)	)	PUNCT
eurjchem-1477	68	13	.	.	PUNCT
eurjchem-1477	69	1	anal	anal	PROPN
eurjchem-1477	69	2	.	.	PUNCT
eurjchem-1477	69	3	calcd	calcd	NOUN
eurjchem-1477	69	4	.	.	PUNCT
eurjchem-1477	70	1	for	for	ADP
eurjchem-1477	70	2	c11h11no	c11h11no	PROPN
eurjchem-1477	70	3	:	:	PUNCT
eurjchem-1477	70	4	c	c	X
eurjchem-1477	70	5	,	,	PUNCT
eurjchem-1477	70	6	76.28	76.28	NUM
eurjchem-1477	70	7	;	;	PUNCT
eurjchem-1477	70	8	h	h	NOUN
eurjchem-1477	70	9	,	,	PUNCT
eurjchem-1477	70	10	6.40	6.40	NUM
eurjchem-1477	70	11	;	;	PUNCT
eurjchem-1477	70	12	n	n	CCONJ
eurjchem-1477	70	13	,	,	PUNCT
eurjchem-1477	70	14	8.09	8.09	NUM
eurjchem-1477	70	15	;	;	PUNCT
eurjchem-1477	70	16	o	o	NOUN
eurjchem-1477	70	17	,	,	PUNCT
eurjchem-1477	70	18	9.24	9.24	NUM
eurjchem-1477	70	19	.	.	PUNCT
eurjchem-1477	71	1	found	find	VERB
eurjchem-1477	71	2	:	:	PUNCT
eurjchem-1477	72	1	c	c	X
eurjchem-1477	72	2	,	,	PUNCT
eurjchem-1477	72	3	76.26	76.26	NUM
eurjchem-1477	72	4	;	;	PUNCT
eurjchem-1477	72	5	h	h	NOUN
eurjchem-1477	72	6	,	,	PUNCT
eurjchem-1477	72	7	6.44	6.44	NUM
eurjchem-1477	72	8	;	;	PUNCT
eurjchem-1477	72	9	n	n	CCONJ
eurjchem-1477	72	10	,	,	PUNCT
eurjchem-1477	72	11	8.06	8.06	NUM
eurjchem-1477	72	12	;	;	PUNCT
eurjchem-1477	72	13	o	o	NOUN
eurjchem-1477	72	14	,	,	PUNCT
eurjchem-1477	72	15	9.22	9.22	NUM
eurjchem-1477	72	16	%	%	NOUN
eurjchem-1477	72	17	.	.	PUNCT
eurjchem-1477	73	1	8‐hydroxy‐1	8‐hydroxy‐1	NUM
eurjchem-1477	73	2	,	,	PUNCT
eurjchem-1477	73	3	3‐dihydro‐benzo[d]azepin‐2‐one	3‐dihydro‐benzo[d]azepin‐2‐one	NUM
eurjchem-1477	73	4	(	(	PUNCT
eurjchem-1477	73	5	3c	3c	NUM
eurjchem-1477	73	6	):	):	PUNCT
eurjchem-1477	73	7	color	color	NOUN
eurjchem-1477	73	8	:	:	PUNCT
eurjchem-1477	73	9	light	light	ADJ
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eurjchem-1477	73	12	.	.	PUNCT
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eurjchem-1477	73	14	:	:	PUNCT
eurjchem-1477	73	15	85	85	NUM
eurjchem-1477	73	16	%	%	NOUN
eurjchem-1477	73	17	.	.	PUNCT
eurjchem-1477	74	1	m.p	m.p	PROPN
eurjchem-1477	74	2	.	.	PROPN
eurjchem-1477	74	3	:	:	PUNCT
eurjchem-1477	75	1	135‐136	135‐136	NUM
eurjchem-1477	75	2	°	°	PROPN
eurjchem-1477	75	3	c	c	PROPN
eurjchem-1477	75	4	.	.	PUNCT
eurjchem-1477	76	1	1h	1h	NUM
eurjchem-1477	76	2	nmr	nmr	NOUN
eurjchem-1477	76	3	(	(	PUNCT
eurjchem-1477	76	4	400	400	NUM
eurjchem-1477	76	5	mhz	mhz	NOUN
eurjchem-1477	76	6	,	,	PUNCT
eurjchem-1477	76	7	cdcl3	cdcl3	PROPN
eurjchem-1477	76	8	,	,	PUNCT
eurjchem-1477	76	9	δ	δ	PROPN
eurjchem-1477	76	10	,	,	PUNCT
eurjchem-1477	76	11	ppm	ppm	NUM
eurjchem-1477	76	12	):	):	PUNCT
eurjchem-1477	76	13	3.44	3.44	NUM
eurjchem-1477	76	14	(	(	PUNCT
eurjchem-1477	76	15	s	s	PROPN
eurjchem-1477	76	16	,	,	PUNCT
eurjchem-1477	76	17	2h	2h	NUM
eurjchem-1477	76	18	,	,	PUNCT
eurjchem-1477	76	19	azepine‐ch2	azepine‐ch2	NUM
eurjchem-1477	76	20	)	)	PUNCT
eurjchem-1477	76	21	,	,	PUNCT
eurjchem-1477	76	22	6.13‐6.12	6.13‐6.12	NUM
eurjchem-1477	76	23	(	(	PUNCT
eurjchem-1477	76	24	d	d	PROPN
eurjchem-1477	76	25	,	,	PUNCT
eurjchem-1477	76	26	1h	1h	NUM
eurjchem-1477	76	27	,	,	PUNCT
eurjchem-1477	76	28	j	j	PROPN
eurjchem-1477	76	29	=	=	SYM
eurjchem-1477	76	30	4.8	4.8	NUM
eurjchem-1477	76	31	hz	hz	VERB
eurjchem-1477	76	32	,	,	PUNCT
eurjchem-1477	76	33	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	76	34	)	)	PUNCT
eurjchem-1477	76	35	,	,	PUNCT
eurjchem-1477	76	36	6.23‐6.20	6.23‐6.20	NUM
eurjchem-1477	76	37	(	(	PUNCT
eurjchem-1477	76	38	d	d	PROPN
eurjchem-1477	76	39	,	,	PUNCT
eurjchem-1477	76	40	1h	1h	NUM
eurjchem-1477	76	41	,	,	PUNCT
eurjchem-1477	76	42	j	j	PROPN
eurjchem-1477	76	43	=	=	SYM
eurjchem-1477	76	44	9.2	9.2	NUM
eurjchem-1477	76	45	hz	hz	VERB
eurjchem-1477	76	46	,	,	PUNCT
eurjchem-1477	76	47	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	76	48	)	)	PUNCT
eurjchem-1477	76	49	,	,	PUNCT
eurjchem-1477	76	50	6.65	6.65	NUM
eurjchem-1477	76	51	(	(	PUNCT
eurjchem-1477	76	52	s	s	PROPN
eurjchem-1477	76	53	,	,	PUNCT
eurjchem-1477	76	54	1h	1h	NUM
eurjchem-1477	76	55	,	,	PUNCT
eurjchem-1477	76	56	ar‐h	ar‐h	NOUN
eurjchem-1477	76	57	)	)	PUNCT
eurjchem-1477	76	58	,	,	PUNCT
eurjchem-1477	76	59	7.10‐7.08	7.10‐7.08	NUM
eurjchem-1477	76	60	(	(	PUNCT
eurjchem-1477	76	61	d	d	PROPN
eurjchem-1477	76	62	,	,	PUNCT
eurjchem-1477	76	63	1h	1h	NUM
eurjchem-1477	76	64	,	,	PUNCT
eurjchem-1477	76	65	j	j	PROPN
eurjchem-1477	77	1	=	=	PROPN
eurjchem-1477	77	2	8.4	8.4	NUM
eurjchem-1477	77	3	hz	hz	NOUN
eurjchem-1477	77	4	,	,	PUNCT
eurjchem-1477	77	5	ar‐	ar‐	PROPN
eurjchem-1477	77	6	h	h	NOUN
eurjchem-1477	77	7	)	)	PUNCT
eurjchem-1477	77	8	,	,	PUNCT
eurjchem-1477	78	1	7.71‐7.69	7.71‐7.69	NUM
eurjchem-1477	78	2	(	(	PUNCT
eurjchem-1477	78	3	d	d	PROPN
eurjchem-1477	78	4	,	,	PUNCT
eurjchem-1477	78	5	1h	1h	NUM
eurjchem-1477	78	6	,	,	PUNCT
eurjchem-1477	78	7	j	j	PROPN
eurjchem-1477	78	8	=	=	SYM
eurjchem-1477	78	9	8	8	NUM
eurjchem-1477	78	10	hz	hz	NOUN
eurjchem-1477	78	11	,	,	PUNCT
eurjchem-1477	78	12	ar‐h	ar‐h	PROPN
eurjchem-1477	78	13	)	)	PUNCT
eurjchem-1477	78	14	,	,	PUNCT
eurjchem-1477	78	15	9.43	9.43	NUM
eurjchem-1477	78	16	(	(	PUNCT
eurjchem-1477	78	17	s	s	PROPN
eurjchem-1477	78	18	,	,	PUNCT
eurjchem-1477	78	19	1h	1h	NUM
eurjchem-1477	78	20	,	,	PUNCT
eurjchem-1477	78	21	nh	nh	PROPN
eurjchem-1477	78	22	)	)	PUNCT
eurjchem-1477	78	23	,	,	PUNCT
eurjchem-1477	78	24	9.57	9.57	NUM
eurjchem-1477	78	25	(	(	PUNCT
eurjchem-1477	78	26	s	s	PROPN
eurjchem-1477	78	27	,	,	PUNCT
eurjchem-1477	78	28	1h	1h	NUM
eurjchem-1477	78	29	,	,	PUNCT
eurjchem-1477	78	30	oh	oh	INTJ
eurjchem-1477	78	31	)	)	PUNCT
eurjchem-1477	78	32	.	.	PUNCT
eurjchem-1477	79	1	13c	13c	NOUN
eurjchem-1477	79	2	nmr	nmr	NOUN
eurjchem-1477	79	3	(	(	PUNCT
eurjchem-1477	79	4	100	100	NUM
eurjchem-1477	79	5	mhz	mhz	NOUN
eurjchem-1477	79	6	,	,	PUNCT
eurjchem-1477	79	7	cdcl3	cdcl3	PROPN
eurjchem-1477	79	8	,	,	PUNCT
eurjchem-1477	79	9	δ	δ	PROPN
eurjchem-1477	79	10	,	,	PUNCT
eurjchem-1477	79	11	ppm	ppm	NOUN
eurjchem-1477	79	12	):	):	PUNCT
eurjchem-1477	79	13	168.41	168.41	NUM
eurjchem-1477	79	14	(	(	PUNCT
eurjchem-1477	79	15	1c	1c	X
eurjchem-1477	79	16	,	,	PUNCT
eurjchem-1477	79	17	conh	conh	NOUN
eurjchem-1477	79	18	)	)	PUNCT
eurjchem-1477	79	19	,	,	PUNCT
eurjchem-1477	79	20	157.74	157.74	NUM
eurjchem-1477	79	21	(	(	PUNCT
eurjchem-1477	79	22	1c	1c	NOUN
eurjchem-1477	79	23	,	,	PUNCT
eurjchem-1477	79	24	ar‐c	ar‐c	PROPN
eurjchem-1477	79	25	)	)	PUNCT
eurjchem-1477	79	26	,	,	PUNCT
eurjchem-1477	79	27	132.35	132.35	NUM
eurjchem-1477	79	28	(	(	PUNCT
eurjchem-1477	79	29	1c	1c	NOUN
eurjchem-1477	79	30	,	,	PUNCT
eurjchem-1477	79	31	ar‐c	ar‐c	PROPN
eurjchem-1477	79	32	)	)	PUNCT
eurjchem-1477	79	33	,	,	PUNCT
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eurjchem-1477	79	35	(	(	PUNCT
eurjchem-1477	79	36	1c	1c	NOUN
eurjchem-1477	79	37	,	,	PUNCT
eurjchem-1477	79	38	ar‐c	ar‐c	PROPN
eurjchem-1477	79	39	)	)	PUNCT
eurjchem-1477	79	40	,	,	PUNCT
eurjchem-1477	79	41	125.76	125.76	NUM
eurjchem-1477	79	42	(	(	PUNCT
eurjchem-1477	79	43	1c	1c	NUM
eurjchem-1477	79	44	,	,	PUNCT
eurjchem-1477	79	45	ar‐c	ar‐c	PROPN
eurjchem-1477	79	46	)	)	PUNCT
eurjchem-1477	79	47	,	,	PUNCT
eurjchem-1477	79	48	123.20	123.20	NUM
eurjchem-1477	79	49	(	(	PUNCT
eurjchem-1477	79	50	1c	1c	NOUN
eurjchem-1477	79	51	,	,	PUNCT
eurjchem-1477	79	52	chnh	chnh	NOUN
eurjchem-1477	79	53	)	)	PUNCT
eurjchem-1477	79	54	,	,	PUNCT
eurjchem-1477	79	55	114.74	114.74	NUM
eurjchem-1477	79	56	(	(	PUNCT
eurjchem-1477	79	57	1c	1c	NOUN
eurjchem-1477	79	58	,	,	PUNCT
eurjchem-1477	79	59	ar‐c	ar‐c	PROPN
eurjchem-1477	79	60	)	)	PUNCT
eurjchem-1477	79	61	,	,	PUNCT
eurjchem-1477	79	62	114.42	114.42	NUM
eurjchem-1477	79	63	(	(	PUNCT
eurjchem-1477	79	64	1c	1c	X
eurjchem-1477	79	65	,	,	PUNCT
eurjchem-1477	79	66	ar‐c	ar‐c	PROPN
eurjchem-1477	79	67	)	)	PUNCT
eurjchem-1477	79	68	,	,	PUNCT
eurjchem-1477	79	69	114.19	114.19	NUM
eurjchem-1477	79	70	(	(	PUNCT
eurjchem-1477	79	71	1c	1c	NOUN
eurjchem-1477	79	72	,	,	PUNCT
eurjchem-1477	79	73	ch‐chnh	ch‐chnh	PROPN
eurjchem-1477	79	74	)	)	PUNCT
eurjchem-1477	79	75	,	,	PUNCT
eurjchem-1477	79	76	43.37	43.37	NUM
eurjchem-1477	79	77	(	(	PUNCT
eurjchem-1477	79	78	1c	1c	NOUN
eurjchem-1477	79	79	,	,	PUNCT
eurjchem-1477	79	80	ch2‐	ch2‐	NOUN
eurjchem-1477	79	81	conh	conh	NOUN
eurjchem-1477	79	82	)	)	PUNCT
eurjchem-1477	79	83	.	.	PUNCT
eurjchem-1477	80	1	ms	ms	NOUN
eurjchem-1477	80	2	(	(	PUNCT
eurjchem-1477	80	3	ei	ei	PROPN
eurjchem-1477	80	4	,	,	PUNCT
eurjchem-1477	80	5	m	m	PROPN
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eurjchem-1477	80	7	z	z	NOUN
eurjchem-1477	80	8	):	):	PUNCT
eurjchem-1477	80	9	176.1877	176.1877	NUM
eurjchem-1477	80	10	(	(	PUNCT
eurjchem-1477	80	11	m+1	m+1	NUM
eurjchem-1477	80	12	)	)	PUNCT
eurjchem-1477	80	13	.	.	PUNCT
eurjchem-1477	81	1	anal	anal	PROPN
eurjchem-1477	81	2	.	.	PUNCT
eurjchem-1477	81	3	calcd	calcd	NOUN
eurjchem-1477	81	4	.	.	PUNCT
eurjchem-1477	82	1	for	for	ADP
eurjchem-1477	82	2	c10h9no2	c10h9no2	PROPN
eurjchem-1477	82	3	:	:	PUNCT
eurjchem-1477	82	4	c	c	X
eurjchem-1477	82	5	,	,	PUNCT
eurjchem-1477	82	6	68.56	68.56	NUM
eurjchem-1477	82	7	;	;	PUNCT
eurjchem-1477	82	8	h	h	NOUN
eurjchem-1477	82	9	,	,	PUNCT
eurjchem-1477	82	10	5.18	5.18	NUM
eurjchem-1477	82	11	;	;	PUNCT
eurjchem-1477	82	12	n	n	CCONJ
eurjchem-1477	82	13	,	,	PUNCT
eurjchem-1477	82	14	8.00	8.00	NUM
eurjchem-1477	82	15	;	;	PUNCT
eurjchem-1477	82	16	o	o	NOUN
eurjchem-1477	82	17	,	,	PUNCT
eurjchem-1477	82	18	18.27	18.27	NUM
eurjchem-1477	82	19	.	.	PUNCT
eurjchem-1477	82	20	found	find	VERB
eurjchem-1477	82	21	:	:	PUNCT
eurjchem-1477	83	1	c	c	X
eurjchem-1477	83	2	,	,	PUNCT
eurjchem-1477	83	3	68.57	68.57	NUM
eurjchem-1477	83	4	;	;	PUNCT
eurjchem-1477	83	5	h	h	NOUN
eurjchem-1477	83	6	,	,	PUNCT
eurjchem-1477	83	7	5.21	5.21	NUM
eurjchem-1477	83	8	;	;	PUNCT
eurjchem-1477	83	9	n	n	CCONJ
eurjchem-1477	83	10	,	,	PUNCT
eurjchem-1477	83	11	8.01	8.01	NUM
eurjchem-1477	83	12	;	;	PUNCT
eurjchem-1477	83	13	o	o	NOUN
eurjchem-1477	83	14	,	,	PUNCT
eurjchem-1477	83	15	18.24	18.24	NUM
eurjchem-1477	83	16	%	%	NOUN
eurjchem-1477	83	17	.	.	PUNCT
eurjchem-1477	84	1	7‐nitro‐1	7‐nitro‐1	NUM
eurjchem-1477	84	2	,	,	PUNCT
eurjchem-1477	84	3	3‐dihydro‐benzo[d]azepin‐2‐one	3‐dihydro‐benzo[d]azepin‐2‐one	NUM
eurjchem-1477	84	4	(	(	PUNCT
eurjchem-1477	84	5	3d	3d	NOUN
eurjchem-1477	84	6	):	):	PUNCT
eurjchem-1477	84	7	color	color	NOUN
eurjchem-1477	84	8	:	:	PUNCT
eurjchem-1477	84	9	light	light	ADJ
eurjchem-1477	84	10	brown	brown	ADJ
eurjchem-1477	84	11	semisolid	semisolid	NOUN
eurjchem-1477	84	12	.	.	PUNCT
eurjchem-1477	85	1	yield	yield	NOUN
eurjchem-1477	85	2	:	:	PUNCT
eurjchem-1477	85	3	93	93	NUM
eurjchem-1477	85	4	%	%	NOUN
eurjchem-1477	85	5	.	.	PUNCT
eurjchem-1477	86	1	m.p	m.p	PROPN
eurjchem-1477	86	2	.	.	PROPN
eurjchem-1477	86	3	:	:	PUNCT
eurjchem-1477	87	1	174‐175	174‐175	NUM
eurjchem-1477	87	2	°	°	PROPN
eurjchem-1477	87	3	c	c	PROPN
eurjchem-1477	87	4	.	.	PUNCT
eurjchem-1477	87	5	1h	1h	NUM
eurjchem-1477	87	6	nmr	nmr	NOUN
eurjchem-1477	87	7	(	(	PUNCT
eurjchem-1477	87	8	400	400	NUM
eurjchem-1477	87	9	mhz	mhz	NOUN
eurjchem-1477	87	10	,	,	PUNCT
eurjchem-1477	87	11	cdcl3	cdcl3	PROPN
eurjchem-1477	87	12	,	,	PUNCT
eurjchem-1477	87	13	δ	δ	PROPN
eurjchem-1477	87	14	,	,	PUNCT
eurjchem-1477	87	15	ppm	ppm	NUM
eurjchem-1477	87	16	):	):	PUNCT
eurjchem-1477	87	17	3.38	3.38	NUM
eurjchem-1477	87	18	(	(	PUNCT
eurjchem-1477	87	19	s	s	PROPN
eurjchem-1477	87	20	,	,	PUNCT
eurjchem-1477	87	21	2h	2h	NUM
eurjchem-1477	87	22	,	,	PUNCT
eurjchem-1477	87	23	azepine‐ch2	azepine‐ch2	NUM
eurjchem-1477	87	24	)	)	PUNCT
eurjchem-1477	87	25	,	,	PUNCT
eurjchem-1477	87	26	6.28‐6.27	6.28‐6.27	NUM
eurjchem-1477	87	27	thimmaiah	thimmaiah	NOUN
eurjchem-1477	87	28	et	et	PROPN
eurjchem-1477	87	29	al	al	PROPN
eurjchem-1477	87	30	.	.	PUNCT
eurjchem-1477	87	31	/	/	SYM
eurjchem-1477	87	32	european	european	PROPN
eurjchem-1477	87	33	journal	journal	PROPN
eurjchem-1477	87	34	of	of	ADP
eurjchem-1477	87	35	chemistry	chemistry	NOUN
eurjchem-1477	87	36	7	7	NUM
eurjchem-1477	87	37	(	(	PUNCT
eurjchem-1477	87	38	4	4	NUM
eurjchem-1477	87	39	)	)	PUNCT
eurjchem-1477	87	40	(	(	PUNCT
eurjchem-1477	87	41	2016	2016	NUM
eurjchem-1477	87	42	)	)	PUNCT
eurjchem-1477	87	43	391‐396	391‐396	NUM
eurjchem-1477	87	44	393	393	NUM
eurjchem-1477	87	45	compound	compound	NOUN
eurjchem-1477	87	46	r	r	NOUN
eurjchem-1477	87	47	3a	3a	NUM
eurjchem-1477	87	48	3‐och3	3‐och3	NUM
eurjchem-1477	87	49	3b	3b	NOUN
eurjchem-1477	87	50	4‐ch3	4‐ch3	NOUN
eurjchem-1477	88	1	3c	3c	NUM
eurjchem-1477	88	2	3‐oh	3‐oh	NUM
eurjchem-1477	88	3	3d	3d	NOUN
eurjchem-1477	88	4	4‐no2	4‐no2	NUM
eurjchem-1477	88	5	3e	3e	NOUN
eurjchem-1477	88	6	4‐f	4‐f	PROPN
eurjchem-1477	88	7	3f	3f	PROPN
eurjchem-1477	88	8	2‐cl	2‐cl	NUM
eurjchem-1477	88	9	3	3	NUM
eurjchem-1477	88	10	g	g	NOUN
eurjchem-1477	88	11	4‐br	4‐br	NUM
eurjchem-1477	88	12	3h	3h	NUM
eurjchem-1477	88	13	3,4‐dichloro	3,4‐dichloro	NUM
eurjchem-1477	88	14	3i	3i	NOUN
eurjchem-1477	88	15	h	h	NOUN
eurjchem-1477	88	16	3j	3j	NOUN
eurjchem-1477	88	17	3‐no2	3‐no2	PRON
eurjchem-1477	88	18	3k	3k	NOUN
eurjchem-1477	88	19	3,4‐dimethoxy	3,4‐dimethoxy	NUM
eurjchem-1477	88	20	scheme	scheme	NOUN
eurjchem-1477	88	21	1	1	NUM
eurjchem-1477	88	22	(	(	PUNCT
eurjchem-1477	88	23	d	d	PROPN
eurjchem-1477	88	24	,	,	PUNCT
eurjchem-1477	88	25	1h	1h	NUM
eurjchem-1477	88	26	,	,	PUNCT
eurjchem-1477	88	27	j	j	PROPN
eurjchem-1477	88	28	=	=	SYM
eurjchem-1477	88	29	4.4	4.4	NUM
eurjchem-1477	88	30	hz	hz	VERB
eurjchem-1477	88	31	,	,	PUNCT
eurjchem-1477	88	32	azapine‐ch	azapine‐ch	ADJ
eurjchem-1477	88	33	)	)	PUNCT
eurjchem-1477	88	34	,	,	PUNCT
eurjchem-1477	88	35	6.44‐6.41	6.44‐6.41	NUM
eurjchem-1477	88	36	(	(	PUNCT
eurjchem-1477	88	37	d	d	PROPN
eurjchem-1477	88	38	,	,	PUNCT
eurjchem-1477	88	39	1h	1h	NUM
eurjchem-1477	88	40	,	,	PUNCT
eurjchem-1477	88	41	j	j	PROPN
eurjchem-1477	89	1	=	=	SYM
eurjchem-1477	89	2	9.1	9.1	NUM
eurjchem-1477	89	3	hz	hz	NOUN
eurjchem-1477	89	4	,	,	PUNCT
eurjchem-1477	89	5	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	89	6	)	)	PUNCT
eurjchem-1477	89	7	,	,	PUNCT
eurjchem-1477	89	8	6.68	6.68	NUM
eurjchem-1477	89	9	(	(	PUNCT
eurjchem-1477	89	10	s	s	PROPN
eurjchem-1477	89	11	,	,	PUNCT
eurjchem-1477	89	12	1h	1h	NUM
eurjchem-1477	89	13	,	,	PUNCT
eurjchem-1477	89	14	ar‐h	ar‐h	NOUN
eurjchem-1477	89	15	)	)	PUNCT
eurjchem-1477	89	16	,	,	PUNCT
eurjchem-1477	89	17	7.20‐7.18	7.20‐7.18	NUM
eurjchem-1477	89	18	(	(	PUNCT
eurjchem-1477	89	19	d	d	PROPN
eurjchem-1477	89	20	,	,	PUNCT
eurjchem-1477	89	21	1h	1h	NUM
eurjchem-1477	89	22	,	,	PUNCT
eurjchem-1477	89	23	j	j	PROPN
eurjchem-1477	90	1	=	=	PROPN
eurjchem-1477	90	2	8.4	8.4	NUM
eurjchem-1477	90	3	hz	hz	NOUN
eurjchem-1477	90	4	,	,	PUNCT
eurjchem-1477	90	5	arh	arh	ADJ
eurjchem-1477	90	6	)	)	PUNCT
eurjchem-1477	90	7	,	,	PUNCT
eurjchem-1477	90	8	7.81‐7.79	7.81‐7.79	NUM
eurjchem-1477	90	9	(	(	PUNCT
eurjchem-1477	90	10	d	d	PROPN
eurjchem-1477	90	11	,	,	PUNCT
eurjchem-1477	90	12	1h	1h	NUM
eurjchem-1477	90	13	,	,	PUNCT
eurjchem-1477	90	14	j	j	PROPN
eurjchem-1477	90	15	=	=	SYM
eurjchem-1477	90	16	8	8	NUM
eurjchem-1477	90	17	hz	hz	NOUN
eurjchem-1477	90	18	,	,	PUNCT
eurjchem-1477	90	19	ar‐h	ar‐h	NOUN
eurjchem-1477	90	20	)	)	PUNCT
eurjchem-1477	90	21	,	,	PUNCT
eurjchem-1477	90	22	9.41	9.41	NUM
eurjchem-1477	90	23	(	(	PUNCT
eurjchem-1477	90	24	s	s	PROPN
eurjchem-1477	90	25	,	,	PUNCT
eurjchem-1477	90	26	1h	1h	NUM
eurjchem-1477	90	27	,	,	PUNCT
eurjchem-1477	90	28	nh	nh	PROPN
eurjchem-1477	90	29	)	)	PUNCT
eurjchem-1477	90	30	.	.	PUNCT
eurjchem-1477	91	1	13c	13c	NOUN
eurjchem-1477	91	2	nmr	nmr	NOUN
eurjchem-1477	91	3	(	(	PUNCT
eurjchem-1477	91	4	100	100	NUM
eurjchem-1477	91	5	mhz	mhz	NOUN
eurjchem-1477	91	6	,	,	PUNCT
eurjchem-1477	91	7	cdcl3	cdcl3	PROPN
eurjchem-1477	91	8	,	,	PUNCT
eurjchem-1477	91	9	δ	δ	PROPN
eurjchem-1477	91	10	,	,	PUNCT
eurjchem-1477	91	11	ppm	ppm	NOUN
eurjchem-1477	91	12	):	):	PUNCT
eurjchem-1477	91	13	168.51	168.51	NUM
eurjchem-1477	91	14	(	(	PUNCT
eurjchem-1477	91	15	1c	1c	X
eurjchem-1477	91	16	,	,	PUNCT
eurjchem-1477	91	17	conh	conh	NOUN
eurjchem-1477	91	18	)	)	PUNCT
eurjchem-1477	91	19	,	,	PUNCT
eurjchem-1477	91	20	157.77	157.77	NUM
eurjchem-1477	91	21	(	(	PUNCT
eurjchem-1477	91	22	1c	1c	NOUN
eurjchem-1477	91	23	,	,	PUNCT
eurjchem-1477	91	24	ar‐c	ar‐c	PROPN
eurjchem-1477	91	25	)	)	PUNCT
eurjchem-1477	91	26	,	,	PUNCT
eurjchem-1477	91	27	132.33	132.33	NUM
eurjchem-1477	91	28	(	(	PUNCT
eurjchem-1477	91	29	1c	1c	NOUN
eurjchem-1477	91	30	,	,	PUNCT
eurjchem-1477	91	31	ar‐c	ar‐c	PROPN
eurjchem-1477	91	32	)	)	PUNCT
eurjchem-1477	91	33	,	,	PUNCT
eurjchem-1477	91	34	127.44	127.44	NUM
eurjchem-1477	91	35	(	(	PUNCT
eurjchem-1477	91	36	1c	1c	NOUN
eurjchem-1477	91	37	,	,	PUNCT
eurjchem-1477	91	38	ar‐c	ar‐c	PROPN
eurjchem-1477	91	39	)	)	PUNCT
eurjchem-1477	91	40	,	,	PUNCT
eurjchem-1477	91	41	125.77	125.77	NUM
eurjchem-1477	91	42	(	(	PUNCT
eurjchem-1477	91	43	1c	1c	NOUN
eurjchem-1477	91	44	,	,	PUNCT
eurjchem-1477	91	45	ar‐c	ar‐c	PROPN
eurjchem-1477	91	46	)	)	PUNCT
eurjchem-1477	91	47	,	,	PUNCT
eurjchem-1477	91	48	123.18	123.18	NUM
eurjchem-1477	91	49	(	(	PUNCT
eurjchem-1477	91	50	1c	1c	NUM
eurjchem-1477	91	51	,	,	PUNCT
eurjchem-1477	91	52	ar‐c	ar‐c	PROPN
eurjchem-1477	91	53	)	)	PUNCT
eurjchem-1477	91	54	,	,	PUNCT
eurjchem-1477	91	55	114.77	114.77	NUM
eurjchem-1477	91	56	(	(	PUNCT
eurjchem-1477	91	57	1c	1c	NOUN
eurjchem-1477	91	58	,	,	PUNCT
eurjchem-1477	91	59	ar‐c	ar‐c	PROPN
eurjchem-1477	91	60	)	)	PUNCT
eurjchem-1477	91	61	,	,	PUNCT
eurjchem-1477	91	62	114.55	114.55	NUM
eurjchem-1477	91	63	(	(	PUNCT
eurjchem-1477	91	64	1c	1c	NOUN
eurjchem-1477	91	65	,	,	PUNCT
eurjchem-1477	91	66	chnh	chnh	NOUN
eurjchem-1477	91	67	)	)	PUNCT
eurjchem-1477	91	68	,	,	PUNCT
eurjchem-1477	91	69	114.21	114.21	NUM
eurjchem-1477	91	70	(	(	PUNCT
eurjchem-1477	91	71	1c	1c	NUM
eurjchem-1477	91	72	,	,	PUNCT
eurjchem-1477	91	73	ch‐chnh	ch‐chnh	PROPN
eurjchem-1477	91	74	)	)	PUNCT
eurjchem-1477	91	75	,	,	PUNCT
eurjchem-1477	91	76	41.37	41.37	NUM
eurjchem-1477	91	77	(	(	PUNCT
eurjchem-1477	91	78	1c	1c	NOUN
eurjchem-1477	91	79	,	,	PUNCT
eurjchem-1477	91	80	ch2‐conh	ch2‐conh	NOUN
eurjchem-1477	91	81	)	)	PUNCT
eurjchem-1477	91	82	.	.	PUNCT
eurjchem-1477	92	1	ms	ms	NOUN
eurjchem-1477	92	2	(	(	PUNCT
eurjchem-1477	92	3	ei	ei	PROPN
eurjchem-1477	92	4	,	,	PUNCT
eurjchem-1477	92	5	m	m	PROPN
eurjchem-1477	92	6	/	/	SYM
eurjchem-1477	92	7	z	z	NOUN
eurjchem-1477	92	8	):	):	PUNCT
eurjchem-1477	92	9	205.1857	205.1857	NUM
eurjchem-1477	92	10	(	(	PUNCT
eurjchem-1477	92	11	m+1	m+1	NUM
eurjchem-1477	92	12	)	)	PUNCT
eurjchem-1477	92	13	.	.	PUNCT
eurjchem-1477	93	1	anal	anal	PROPN
eurjchem-1477	93	2	.	.	PUNCT
eurjchem-1477	93	3	calcd	calcd	NOUN
eurjchem-1477	93	4	.	.	PUNCT
eurjchem-1477	94	1	for	for	ADP
eurjchem-1477	94	2	c10h8n2o3	c10h8n2o3	NOUN
eurjchem-1477	94	3	:	:	PUNCT
eurjchem-1477	94	4	c	c	X
eurjchem-1477	94	5	,	,	PUNCT
eurjchem-1477	94	6	58.82	58.82	NUM
eurjchem-1477	94	7	;	;	PUNCT
eurjchem-1477	94	8	h	h	NOUN
eurjchem-1477	94	9	,	,	PUNCT
eurjchem-1477	94	10	3.95	3.95	NUM
eurjchem-1477	94	11	;	;	PUNCT
eurjchem-1477	94	12	n	n	CCONJ
eurjchem-1477	94	13	,	,	PUNCT
eurjchem-1477	94	14	13.72	13.72	NUM
eurjchem-1477	94	15	;	;	PUNCT
eurjchem-1477	94	16	o	o	NOUN
eurjchem-1477	94	17	,	,	PUNCT
eurjchem-1477	94	18	23.51	23.51	NUM
eurjchem-1477	94	19	.	.	PUNCT
eurjchem-1477	95	1	found	find	VERB
eurjchem-1477	95	2	:	:	PUNCT
eurjchem-1477	96	1	c	c	X
eurjchem-1477	96	2	,	,	PUNCT
eurjchem-1477	96	3	58.81	58.81	NUM
eurjchem-1477	96	4	;	;	PUNCT
eurjchem-1477	96	5	h	h	X
eurjchem-1477	96	6	,	,	PUNCT
eurjchem-1477	96	7	3.97	3.97	NUM
eurjchem-1477	96	8	;	;	PUNCT
eurjchem-1477	96	9	n	n	CCONJ
eurjchem-1477	96	10	,	,	PUNCT
eurjchem-1477	96	11	13.76	13.76	NUM
eurjchem-1477	96	12	;	;	PUNCT
eurjchem-1477	96	13	o	o	NOUN
eurjchem-1477	96	14	,	,	PUNCT
eurjchem-1477	96	15	23.50	23.50	NUM
eurjchem-1477	96	16	%	%	NOUN
eurjchem-1477	96	17	.	.	PUNCT
eurjchem-1477	97	1	7‐fluoro‐1	7‐fluoro‐1	NUM
eurjchem-1477	97	2	,	,	PUNCT
eurjchem-1477	97	3	3‐dihydro‐benzo[d]azepin‐2‐one	3‐dihydro‐benzo[d]azepin‐2‐one	NUM
eurjchem-1477	97	4	(	(	PUNCT
eurjchem-1477	97	5	3e	3e	NUM
eurjchem-1477	97	6	):	):	PUNCT
eurjchem-1477	97	7	color	color	NOUN
eurjchem-1477	97	8	:	:	PUNCT
eurjchem-1477	97	9	light	light	ADJ
eurjchem-1477	97	10	yellow	yellow	ADJ
eurjchem-1477	97	11	semisolid	semisolid	NOUN
eurjchem-1477	97	12	.	.	PUNCT
eurjchem-1477	98	1	yield	yield	NOUN
eurjchem-1477	98	2	:	:	PUNCT
eurjchem-1477	98	3	92	92	NUM
eurjchem-1477	98	4	%	%	NOUN
eurjchem-1477	98	5	.	.	PUNCT
eurjchem-1477	99	1	m.p	m.p	PROPN
eurjchem-1477	99	2	.	.	PROPN
eurjchem-1477	99	3	:	:	PUNCT
eurjchem-1477	100	1	104‐106	104‐106	NUM
eurjchem-1477	100	2	°	°	SYM
eurjchem-1477	100	3	c	c	NOUN
eurjchem-1477	100	4	.	.	PUNCT
eurjchem-1477	101	1	1h	1h	NUM
eurjchem-1477	101	2	nmr	nmr	NOUN
eurjchem-1477	101	3	(	(	PUNCT
eurjchem-1477	101	4	400	400	NUM
eurjchem-1477	101	5	mhz	mhz	NOUN
eurjchem-1477	101	6	,	,	PUNCT
eurjchem-1477	101	7	cdcl3	cdcl3	PROPN
eurjchem-1477	101	8	,	,	PUNCT
eurjchem-1477	101	9	δ	δ	PROPN
eurjchem-1477	101	10	,	,	PUNCT
eurjchem-1477	101	11	ppm	ppm	NUM
eurjchem-1477	101	12	):	):	PUNCT
eurjchem-1477	101	13	3.34	3.34	NUM
eurjchem-1477	101	14	(	(	PUNCT
eurjchem-1477	101	15	s	s	PROPN
eurjchem-1477	101	16	,	,	PUNCT
eurjchem-1477	101	17	2h	2h	NUM
eurjchem-1477	101	18	,	,	PUNCT
eurjchem-1477	101	19	azepine‐ch2	azepine‐ch2	NUM
eurjchem-1477	101	20	)	)	PUNCT
eurjchem-1477	101	21	,	,	PUNCT
eurjchem-1477	101	22	6.18‐6.19	6.18‐6.19	NUM
eurjchem-1477	101	23	(	(	PUNCT
eurjchem-1477	101	24	d	d	PROPN
eurjchem-1477	101	25	,	,	PUNCT
eurjchem-1477	101	26	1h	1h	NUM
eurjchem-1477	101	27	,	,	PUNCT
eurjchem-1477	101	28	j	j	PROPN
eurjchem-1477	101	29	=	=	SYM
eurjchem-1477	101	30	4.8	4.8	NUM
eurjchem-1477	101	31	hz	hz	VERB
eurjchem-1477	101	32	,	,	PUNCT
eurjchem-1477	101	33	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	101	34	)	)	PUNCT
eurjchem-1477	101	35	,	,	PUNCT
eurjchem-1477	101	36	6.33‐6.30	6.33‐6.30	NUM
eurjchem-1477	101	37	(	(	PUNCT
eurjchem-1477	101	38	d	d	PROPN
eurjchem-1477	101	39	,	,	PUNCT
eurjchem-1477	101	40	1h	1h	NUM
eurjchem-1477	101	41	,	,	PUNCT
eurjchem-1477	101	42	j	j	PROPN
eurjchem-1477	102	1	=	=	SYM
eurjchem-1477	102	2	9.0	9.0	NUM
eurjchem-1477	102	3	hz	hz	VERB
eurjchem-1477	102	4	,	,	PUNCT
eurjchem-1477	102	5	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	102	6	)	)	PUNCT
eurjchem-1477	102	7	,	,	PUNCT
eurjchem-1477	102	8	6.90	6.90	NUM
eurjchem-1477	102	9	(	(	PUNCT
eurjchem-1477	102	10	s	s	PROPN
eurjchem-1477	102	11	,	,	PUNCT
eurjchem-1477	102	12	1h	1h	NUM
eurjchem-1477	102	13	,	,	PUNCT
eurjchem-1477	102	14	ar‐h	ar‐h	NOUN
eurjchem-1477	102	15	)	)	PUNCT
eurjchem-1477	102	16	,	,	PUNCT
eurjchem-1477	102	17	6.88‐6.87	6.88‐6.87	NUM
eurjchem-1477	102	18	(	(	PUNCT
eurjchem-1477	102	19	d	d	PROPN
eurjchem-1477	102	20	,	,	PUNCT
eurjchem-1477	102	21	1h	1h	NUM
eurjchem-1477	102	22	,	,	PUNCT
eurjchem-1477	102	23	j	j	PROPN
eurjchem-1477	103	1	=	=	SYM
eurjchem-1477	103	2	7.2	7.2	NUM
eurjchem-1477	103	3	hz	hz	NOUN
eurjchem-1477	103	4	,	,	PUNCT
eurjchem-1477	103	5	ar‐	ar‐	PROPN
eurjchem-1477	103	6	h	h	NOUN
eurjchem-1477	103	7	)	)	PUNCT
eurjchem-1477	103	8	,	,	PUNCT
eurjchem-1477	103	9	6.96‐6.98	6.96‐6.98	NUM
eurjchem-1477	103	10	(	(	PUNCT
eurjchem-1477	103	11	d	d	PROPN
eurjchem-1477	103	12	,	,	PUNCT
eurjchem-1477	103	13	1h	1h	NUM
eurjchem-1477	103	14	,	,	PUNCT
eurjchem-1477	103	15	j	j	PROPN
eurjchem-1477	103	16	=	=	PROPN
eurjchem-1477	103	17	8.8	8.8	NUM
eurjchem-1477	103	18	hz	hz	NOUN
eurjchem-1477	103	19	,	,	PUNCT
eurjchem-1477	103	20	ar‐h	ar‐h	PROPN
eurjchem-1477	103	21	)	)	PUNCT
eurjchem-1477	103	22	,	,	PUNCT
eurjchem-1477	103	23	9.44	9.44	NUM
eurjchem-1477	103	24	(	(	PUNCT
eurjchem-1477	103	25	s	s	PROPN
eurjchem-1477	103	26	,	,	PUNCT
eurjchem-1477	103	27	1h	1h	NUM
eurjchem-1477	103	28	,	,	PUNCT
eurjchem-1477	103	29	nh	nh	PROPN
eurjchem-1477	103	30	)	)	PUNCT
eurjchem-1477	103	31	.	.	PUNCT
eurjchem-1477	104	1	13c	13c	NOUN
eurjchem-1477	104	2	nmr	nmr	NOUN
eurjchem-1477	104	3	(	(	PUNCT
eurjchem-1477	104	4	100	100	NUM
eurjchem-1477	104	5	mhz	mhz	NOUN
eurjchem-1477	104	6	,	,	PUNCT
eurjchem-1477	104	7	cdcl3	cdcl3	PROPN
eurjchem-1477	104	8	,	,	PUNCT
eurjchem-1477	104	9	δ	δ	PROPN
eurjchem-1477	104	10	,	,	PUNCT
eurjchem-1477	104	11	ppm	ppm	NUM
eurjchem-1477	104	12	):	):	PUNCT
eurjchem-1477	104	13	170.32	170.32	NUM
eurjchem-1477	104	14	(	(	PUNCT
eurjchem-1477	104	15	1c	1c	NOUN
eurjchem-1477	104	16	,	,	PUNCT
eurjchem-1477	104	17	conh	conh	NOUN
eurjchem-1477	104	18	)	)	PUNCT
eurjchem-1477	104	19	,	,	PUNCT
eurjchem-1477	104	20	161.54	161.54	NUM
eurjchem-1477	104	21	(	(	PUNCT
eurjchem-1477	104	22	1c	1c	X
eurjchem-1477	104	23	,	,	PUNCT
eurjchem-1477	104	24	ar‐	ar‐	NOUN
eurjchem-1477	104	25	c	c	X
eurjchem-1477	104	26	)	)	PUNCT
eurjchem-1477	104	27	,	,	PUNCT
eurjchem-1477	104	28	132.45	132.45	NUM
eurjchem-1477	104	29	(	(	PUNCT
eurjchem-1477	104	30	1c	1c	NUM
eurjchem-1477	104	31	,	,	PUNCT
eurjchem-1477	104	32	ar‐c	ar‐c	PROPN
eurjchem-1477	104	33	)	)	PUNCT
eurjchem-1477	104	34	,	,	PUNCT
eurjchem-1477	104	35	128.14	128.14	NUM
eurjchem-1477	104	36	(	(	PUNCT
eurjchem-1477	104	37	1c	1c	NOUN
eurjchem-1477	104	38	,	,	PUNCT
eurjchem-1477	104	39	ar‐c	ar‐c	PROPN
eurjchem-1477	104	40	)	)	PUNCT
eurjchem-1477	104	41	,	,	PUNCT
eurjchem-1477	104	42	127.30	127.30	NUM
eurjchem-1477	104	43	(	(	PUNCT
eurjchem-1477	104	44	1c	1c	NUM
eurjchem-1477	104	45	,	,	PUNCT
eurjchem-1477	104	46	ar‐c	ar‐c	PROPN
eurjchem-1477	104	47	)	)	PUNCT
eurjchem-1477	104	48	,	,	PUNCT
eurjchem-1477	104	49	122.77	122.77	NUM
eurjchem-1477	104	50	(	(	PUNCT
eurjchem-1477	104	51	1c	1c	NOUN
eurjchem-1477	104	52	,	,	PUNCT
eurjchem-1477	104	53	chnh	chnh	NOUN
eurjchem-1477	104	54	)	)	PUNCT
eurjchem-1477	104	55	,	,	PUNCT
eurjchem-1477	104	56	116.62	116.62	NUM
eurjchem-1477	104	57	(	(	PUNCT
eurjchem-1477	104	58	1c	1c	NOUN
eurjchem-1477	104	59	,	,	PUNCT
eurjchem-1477	104	60	ar‐c	ar‐c	PROPN
eurjchem-1477	104	61	)	)	PUNCT
eurjchem-1477	104	62	,	,	PUNCT
eurjchem-1477	104	63	113.99	113.99	NUM
eurjchem-1477	104	64	(	(	PUNCT
eurjchem-1477	104	65	1c	1c	NOUN
eurjchem-1477	104	66	,	,	PUNCT
eurjchem-1477	104	67	ar‐c	ar‐c	PROPN
eurjchem-1477	104	68	)	)	PUNCT
eurjchem-1477	104	69	,	,	PUNCT
eurjchem-1477	104	70	113.46	113.46	NUM
eurjchem-1477	104	71	(	(	PUNCT
eurjchem-1477	104	72	1c	1c	NUM
eurjchem-1477	104	73	,	,	PUNCT
eurjchem-1477	104	74	ch‐chnh	ch‐chnh	PROPN
eurjchem-1477	104	75	)	)	PUNCT
eurjchem-1477	104	76	,	,	PUNCT
eurjchem-1477	104	77	43.62	43.62	NUM
eurjchem-1477	104	78	(	(	PUNCT
eurjchem-1477	104	79	1c	1c	NOUN
eurjchem-1477	104	80	,	,	PUNCT
eurjchem-1477	104	81	ch2‐conh	ch2‐conh	NOUN
eurjchem-1477	104	82	)	)	PUNCT
eurjchem-1477	104	83	.	.	PUNCT
eurjchem-1477	105	1	ms	ms	NOUN
eurjchem-1477	105	2	(	(	PUNCT
eurjchem-1477	105	3	ei	ei	PROPN
eurjchem-1477	105	4	,	,	PUNCT
eurjchem-1477	105	5	m	m	PROPN
eurjchem-1477	105	6	/	/	SYM
eurjchem-1477	105	7	z	z	NOUN
eurjchem-1477	105	8	):	):	PUNCT
eurjchem-1477	105	9	178.1867	178.1867	NUM
eurjchem-1477	105	10	(	(	PUNCT
eurjchem-1477	105	11	m+1	m+1	NUM
eurjchem-1477	105	12	)	)	PUNCT
eurjchem-1477	105	13	.	.	PUNCT
eurjchem-1477	106	1	anal	anal	PROPN
eurjchem-1477	106	2	.	.	PUNCT
eurjchem-1477	106	3	calcd	calcd	NOUN
eurjchem-1477	106	4	.	.	PUNCT
eurjchem-1477	107	1	for	for	ADP
eurjchem-1477	107	2	c10h8fno	c10h8fno	PROPN
eurjchem-1477	107	3	:	:	PUNCT
eurjchem-1477	107	4	c	c	X
eurjchem-1477	107	5	,	,	PUNCT
eurjchem-1477	107	6	67.79	67.79	NUM
eurjchem-1477	107	7	;	;	PUNCT
eurjchem-1477	107	8	h	h	NOUN
eurjchem-1477	107	9	,	,	PUNCT
eurjchem-1477	107	10	4.55	4.55	NUM
eurjchem-1477	107	11	;	;	PUNCT
eurjchem-1477	107	12	n	n	CCONJ
eurjchem-1477	107	13	,	,	PUNCT
eurjchem-1477	107	14	7.91	7.91	NUM
eurjchem-1477	107	15	;	;	PUNCT
eurjchem-1477	107	16	o	o	NOUN
eurjchem-1477	107	17	,	,	PUNCT
eurjchem-1477	107	18	9.03	9.03	NUM
eurjchem-1477	107	19	.	.	PUNCT
eurjchem-1477	107	20	found	find	VERB
eurjchem-1477	107	21	:	:	PUNCT
eurjchem-1477	108	1	c	c	X
eurjchem-1477	108	2	,	,	PUNCT
eurjchem-1477	108	3	67.77	67.77	NUM
eurjchem-1477	108	4	;	;	PUNCT
eurjchem-1477	108	5	h	h	NOUN
eurjchem-1477	108	6	,	,	PUNCT
eurjchem-1477	108	7	4.53	4.53	NUM
eurjchem-1477	108	8	;	;	PUNCT
eurjchem-1477	108	9	n	n	CCONJ
eurjchem-1477	108	10	,	,	PUNCT
eurjchem-1477	108	11	7.95	7.95	NUM
eurjchem-1477	108	12	;	;	PUNCT
eurjchem-1477	108	13	o	o	NOUN
eurjchem-1477	108	14	,	,	PUNCT
eurjchem-1477	108	15	9.01	9.01	NUM
eurjchem-1477	108	16	%	%	NOUN
eurjchem-1477	108	17	.	.	PUNCT
eurjchem-1477	109	1	9‐chloro‐1	9‐chloro‐1	NUM
eurjchem-1477	109	2	,	,	PUNCT
eurjchem-1477	109	3	3‐dihydro‐benzo[d]azepin‐2‐one	3‐dihydro‐benzo[d]azepin‐2‐one	NUM
eurjchem-1477	109	4	(	(	PUNCT
eurjchem-1477	109	5	3f	3f	NUM
eurjchem-1477	109	6	):	):	PUNCT
eurjchem-1477	109	7	color	color	NOUN
eurjchem-1477	109	8	:	:	PUNCT
eurjchem-1477	109	9	brown	brown	ADJ
eurjchem-1477	109	10	semisolid	semisolid	NOUN
eurjchem-1477	109	11	.	.	PUNCT
eurjchem-1477	110	1	yield	yield	NOUN
eurjchem-1477	110	2	:	:	PUNCT
eurjchem-1477	110	3	90	90	NUM
eurjchem-1477	110	4	%	%	NOUN
eurjchem-1477	110	5	.	.	PUNCT
eurjchem-1477	111	1	m.p	m.p	PROPN
eurjchem-1477	111	2	.	.	PROPN
eurjchem-1477	111	3	:	:	PUNCT
eurjchem-1477	112	1	133‐135	133‐135	NUM
eurjchem-1477	112	2	°	°	SYM
eurjchem-1477	112	3	c	c	NOUN
eurjchem-1477	112	4	.	.	PUNCT
eurjchem-1477	112	5	1h	1h	NUM
eurjchem-1477	112	6	nmr	nmr	NOUN
eurjchem-1477	112	7	(	(	PUNCT
eurjchem-1477	112	8	400	400	NUM
eurjchem-1477	112	9	mhz	mhz	NOUN
eurjchem-1477	112	10	,	,	PUNCT
eurjchem-1477	112	11	cdcl3	cdcl3	PROPN
eurjchem-1477	112	12	,	,	PUNCT
eurjchem-1477	112	13	δ	δ	PROPN
eurjchem-1477	112	14	,	,	PUNCT
eurjchem-1477	112	15	ppm	ppm	NUM
eurjchem-1477	112	16	):	):	PUNCT
eurjchem-1477	112	17	3.25	3.25	NUM
eurjchem-1477	112	18	(	(	PUNCT
eurjchem-1477	112	19	s	s	PROPN
eurjchem-1477	112	20	,	,	PUNCT
eurjchem-1477	112	21	2h	2h	NUM
eurjchem-1477	112	22	,	,	PUNCT
eurjchem-1477	112	23	azepine‐ch2	azepine‐ch2	NUM
eurjchem-1477	112	24	)	)	PUNCT
eurjchem-1477	112	25	,	,	PUNCT
eurjchem-1477	112	26	6.15‐6.13	6.15‐6.13	NUM
eurjchem-1477	112	27	(	(	PUNCT
eurjchem-1477	112	28	d	d	PROPN
eurjchem-1477	112	29	,	,	PUNCT
eurjchem-1477	112	30	1h	1h	NUM
eurjchem-1477	112	31	,	,	PUNCT
eurjchem-1477	112	32	j	j	PROPN
eurjchem-1477	112	33	=	=	PROPN
eurjchem-1477	112	34	8.4	8.4	NUM
eurjchem-1477	112	35	hz	hz	NOUN
eurjchem-1477	112	36	,	,	PUNCT
eurjchem-1477	112	37	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	112	38	)	)	PUNCT
eurjchem-1477	112	39	,	,	PUNCT
eurjchem-1477	113	1	7.23‐7.22	7.23‐7.22	NUM
eurjchem-1477	113	2	(	(	PUNCT
eurjchem-1477	113	3	d	d	PROPN
eurjchem-1477	113	4	,	,	PUNCT
eurjchem-1477	113	5	1h	1h	NUM
eurjchem-1477	113	6	,	,	PUNCT
eurjchem-1477	113	7	j	j	PROPN
eurjchem-1477	113	8	=	=	SYM
eurjchem-1477	113	9	4.4	4.4	NUM
eurjchem-1477	113	10	hz	hz	VERB
eurjchem-1477	113	11	,	,	PUNCT
eurjchem-1477	113	12	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	113	13	)	)	PUNCT
eurjchem-1477	113	14	,	,	PUNCT
eurjchem-1477	113	15	6.98‐6.98	6.98‐6.98	NUM
eurjchem-1477	113	16	(	(	PUNCT
eurjchem-1477	113	17	t	t	PROPN
eurjchem-1477	113	18	,	,	PUNCT
eurjchem-1477	113	19	1h	1h	NUM
eurjchem-1477	113	20	,	,	PUNCT
eurjchem-1477	113	21	j	j	PROPN
eurjchem-1477	113	22	=	=	SYM
eurjchem-1477	113	23	2.8	2.8	NUM
eurjchem-1477	113	24	hz	hz	ADJ
eurjchem-1477	113	25	,	,	PUNCT
eurjchem-1477	113	26	ar‐h	ar‐h	PROPN
eurjchem-1477	113	27	)	)	PUNCT
eurjchem-1477	113	28	,	,	PUNCT
eurjchem-1477	113	29	7.13‐7.14	7.13‐7.14	NUM
eurjchem-1477	113	30	(	(	PUNCT
eurjchem-1477	113	31	d	d	PROPN
eurjchem-1477	113	32	,	,	PUNCT
eurjchem-1477	113	33	1h	1h	NUM
eurjchem-1477	113	34	,	,	PUNCT
eurjchem-1477	113	35	j	j	PROPN
eurjchem-1477	113	36	=	=	SYM
eurjchem-1477	113	37	4.8	4.8	NUM
eurjchem-1477	113	38	hz	hz	VERB
eurjchem-1477	113	39	,	,	PUNCT
eurjchem-1477	113	40	ar‐h	ar‐h	NOUN
eurjchem-1477	113	41	)	)	PUNCT
eurjchem-1477	113	42	,	,	PUNCT
eurjchem-1477	113	43	7.23‐7.25	7.23‐7.25	NUM
eurjchem-1477	113	44	(	(	PUNCT
eurjchem-1477	113	45	d	d	PROPN
eurjchem-1477	113	46	,	,	PUNCT
eurjchem-1477	113	47	1h	1h	NUM
eurjchem-1477	113	48	,	,	PUNCT
eurjchem-1477	113	49	j	j	PROPN
eurjchem-1477	113	50	=	=	SYM
eurjchem-1477	113	51	7.6	7.6	NUM
eurjchem-1477	113	52	hz	hz	NOUN
eurjchem-1477	113	53	,	,	PUNCT
eurjchem-1477	113	54	ar‐h	ar‐h	NOUN
eurjchem-1477	113	55	)	)	PUNCT
eurjchem-1477	113	56	,	,	PUNCT
eurjchem-1477	113	57	9.41	9.41	NUM
eurjchem-1477	113	58	(	(	PUNCT
eurjchem-1477	113	59	s	s	PROPN
eurjchem-1477	113	60	,	,	PUNCT
eurjchem-1477	113	61	1h	1h	NUM
eurjchem-1477	113	62	,	,	PUNCT
eurjchem-1477	113	63	nh	nh	PROPN
eurjchem-1477	113	64	)	)	PUNCT
eurjchem-1477	113	65	.	.	PUNCT
eurjchem-1477	114	1	13c	13c	NOUN
eurjchem-1477	114	2	nmr	nmr	NOUN
eurjchem-1477	114	3	(	(	PUNCT
eurjchem-1477	114	4	100	100	NUM
eurjchem-1477	114	5	mhz	mhz	NOUN
eurjchem-1477	114	6	,	,	PUNCT
eurjchem-1477	114	7	cdcl3	cdcl3	PROPN
eurjchem-1477	114	8	,	,	PUNCT
eurjchem-1477	114	9	δ	δ	PROPN
eurjchem-1477	114	10	,	,	PUNCT
eurjchem-1477	114	11	ppm	ppm	NUM
eurjchem-1477	114	12	):	):	PUNCT
eurjchem-1477	114	13	169.32	169.32	NUM
eurjchem-1477	114	14	(	(	PUNCT
eurjchem-1477	114	15	1c	1c	X
eurjchem-1477	114	16	,	,	PUNCT
eurjchem-1477	114	17	conh	conh	NOUN
eurjchem-1477	114	18	)	)	PUNCT
eurjchem-1477	114	19	,	,	PUNCT
eurjchem-1477	114	20	160.53	160.53	NUM
eurjchem-1477	114	21	(	(	PUNCT
eurjchem-1477	114	22	1c	1c	NUM
eurjchem-1477	114	23	,	,	PUNCT
eurjchem-1477	114	24	ar‐c	ar‐c	PROPN
eurjchem-1477	114	25	)	)	PUNCT
eurjchem-1477	114	26	,	,	PUNCT
eurjchem-1477	114	27	132.75	132.75	NUM
eurjchem-1477	114	28	(	(	PUNCT
eurjchem-1477	114	29	1c	1c	NOUN
eurjchem-1477	114	30	,	,	PUNCT
eurjchem-1477	114	31	ar‐c	ar‐c	PROPN
eurjchem-1477	114	32	)	)	PUNCT
eurjchem-1477	114	33	,	,	PUNCT
eurjchem-1477	114	34	128.11	128.11	NUM
eurjchem-1477	114	35	(	(	PUNCT
eurjchem-1477	114	36	1c	1c	NOUN
eurjchem-1477	114	37	,	,	PUNCT
eurjchem-1477	114	38	ar‐c	ar‐c	PROPN
eurjchem-1477	114	39	)	)	PUNCT
eurjchem-1477	114	40	,	,	PUNCT
eurjchem-1477	114	41	127.55	127.55	NUM
eurjchem-1477	114	42	(	(	PUNCT
eurjchem-1477	114	43	1c	1c	NOUN
eurjchem-1477	114	44	,	,	PUNCT
eurjchem-1477	114	45	ar‐c	ar‐c	PROPN
eurjchem-1477	114	46	)	)	PUNCT
eurjchem-1477	114	47	,	,	PUNCT
eurjchem-1477	114	48	123.77	123.77	NUM
eurjchem-1477	114	49	(	(	PUNCT
eurjchem-1477	114	50	1c	1c	NOUN
eurjchem-1477	114	51	,	,	PUNCT
eurjchem-1477	114	52	ar‐c	ar‐c	PROPN
eurjchem-1477	114	53	)	)	PUNCT
eurjchem-1477	114	54	,	,	PUNCT
eurjchem-1477	114	55	116.41	116.41	NUM
eurjchem-1477	114	56	(	(	PUNCT
eurjchem-1477	114	57	1c	1c	NOUN
eurjchem-1477	114	58	,	,	PUNCT
eurjchem-1477	114	59	ar‐c	ar‐c	PROPN
eurjchem-1477	114	60	)	)	PUNCT
eurjchem-1477	114	61	,	,	PUNCT
eurjchem-1477	114	62	113.91	113.91	NUM
eurjchem-1477	114	63	(	(	PUNCT
eurjchem-1477	114	64	1c	1c	X
eurjchem-1477	114	65	,	,	PUNCT
eurjchem-1477	114	66	chnh	chnh	NOUN
eurjchem-1477	114	67	)	)	PUNCT
eurjchem-1477	114	68	,	,	PUNCT
eurjchem-1477	114	69	113.22	113.22	NUM
eurjchem-1477	114	70	(	(	PUNCT
eurjchem-1477	114	71	1c	1c	NOUN
eurjchem-1477	114	72	,	,	PUNCT
eurjchem-1477	114	73	ch‐chnh	ch‐chnh	PROPN
eurjchem-1477	114	74	)	)	PUNCT
eurjchem-1477	114	75	,	,	PUNCT
eurjchem-1477	114	76	42.62	42.62	NUM
eurjchem-1477	114	77	(	(	PUNCT
eurjchem-1477	114	78	1c	1c	NOUN
eurjchem-1477	114	79	,	,	PUNCT
eurjchem-1477	114	80	ch2‐conh	ch2‐conh	NOUN
eurjchem-1477	114	81	)	)	PUNCT
eurjchem-1477	114	82	.	.	PUNCT
eurjchem-1477	115	1	ms	ms	NOUN
eurjchem-1477	115	2	(	(	PUNCT
eurjchem-1477	115	3	ei	ei	PROPN
eurjchem-1477	115	4	,	,	PUNCT
eurjchem-1477	115	5	m	m	PROPN
eurjchem-1477	115	6	/	/	SYM
eurjchem-1477	115	7	z	z	NOUN
eurjchem-1477	115	8	):	):	PUNCT
eurjchem-1477	115	9	193.6322	193.6322	NUM
eurjchem-1477	115	10	(	(	PUNCT
eurjchem-1477	115	11	m+	m+	NUM
eurjchem-1477	115	12	)	)	PUNCT
eurjchem-1477	115	13	.	.	PUNCT
eurjchem-1477	116	1	anal	anal	PROPN
eurjchem-1477	116	2	.	.	PUNCT
eurjchem-1477	116	3	calcd	calcd	NOUN
eurjchem-1477	116	4	.	.	PUNCT
eurjchem-1477	117	1	for	for	ADP
eurjchem-1477	117	2	c10h8clno	c10h8clno	PROPN
eurjchem-1477	117	3	:	:	PUNCT
eurjchem-1477	117	4	c	c	X
eurjchem-1477	117	5	,	,	PUNCT
eurjchem-1477	117	6	62.03	62.03	NUM
eurjchem-1477	117	7	;	;	PUNCT
eurjchem-1477	117	8	h	h	X
eurjchem-1477	117	9	,	,	PUNCT
eurjchem-1477	117	10	4.16	4.16	NUM
eurjchem-1477	117	11	;	;	PUNCT
eurjchem-1477	117	12	n	n	CCONJ
eurjchem-1477	117	13	,	,	PUNCT
eurjchem-1477	117	14	7.23	7.23	NUM
eurjchem-1477	117	15	;	;	PUNCT
eurjchem-1477	117	16	o	o	NOUN
eurjchem-1477	117	17	,	,	PUNCT
eurjchem-1477	117	18	8.26	8.26	NUM
eurjchem-1477	117	19	.	.	PUNCT
eurjchem-1477	117	20	found	find	VERB
eurjchem-1477	117	21	:	:	PUNCT
eurjchem-1477	118	1	c	c	X
eurjchem-1477	118	2	,	,	PUNCT
eurjchem-1477	118	3	62.01	62.01	NUM
eurjchem-1477	118	4	;	;	PUNCT
eurjchem-1477	118	5	h	h	X
eurjchem-1477	118	6	,	,	PUNCT
eurjchem-1477	118	7	4.17	4.17	NUM
eurjchem-1477	118	8	;	;	PUNCT
eurjchem-1477	118	9	n	n	CCONJ
eurjchem-1477	118	10	,	,	PUNCT
eurjchem-1477	118	11	7.26	7.26	NUM
eurjchem-1477	118	12	;	;	PUNCT
eurjchem-1477	118	13	o	o	X
eurjchem-1477	118	14	,	,	PUNCT
eurjchem-1477	118	15	8.22	8.22	NUM
eurjchem-1477	118	16	%	%	NOUN
eurjchem-1477	118	17	.	.	PUNCT
eurjchem-1477	119	1	7‐bromo‐1	7‐bromo‐1	ADV
eurjchem-1477	119	2	,	,	PUNCT
eurjchem-1477	119	3	3‐dihydro‐benzo[d]azepin‐2‐one	3‐dihydro‐benzo[d]azepin‐2‐one	NUM
eurjchem-1477	119	4	(	(	PUNCT
eurjchem-1477	119	5	3	3	NUM
eurjchem-1477	119	6	g	g	NOUN
eurjchem-1477	119	7	):	):	PUNCT
eurjchem-1477	119	8	color	color	NOUN
eurjchem-1477	119	9	:	:	PUNCT
eurjchem-1477	119	10	pale	pale	ADJ
eurjchem-1477	119	11	yellow	yellow	ADJ
eurjchem-1477	119	12	semi	semi	ADV
eurjchem-1477	119	13	solid	solid	ADJ
eurjchem-1477	119	14	.	.	PUNCT
eurjchem-1477	120	1	yield	yield	NOUN
eurjchem-1477	120	2	:	:	PUNCT
eurjchem-1477	120	3	92	92	NUM
eurjchem-1477	120	4	%	%	NOUN
eurjchem-1477	120	5	.	.	PUNCT
eurjchem-1477	121	1	m.p	m.p	PROPN
eurjchem-1477	121	2	.	.	PROPN
eurjchem-1477	121	3	:	:	PUNCT
eurjchem-1477	122	1	163‐165	163‐165	NUM
eurjchem-1477	122	2	°	°	PROPN
eurjchem-1477	122	3	c	c	PROPN
eurjchem-1477	122	4	.	.	PUNCT
eurjchem-1477	123	1	1h	1h	NUM
eurjchem-1477	123	2	nmr	nmr	NOUN
eurjchem-1477	123	3	(	(	PUNCT
eurjchem-1477	123	4	400	400	NUM
eurjchem-1477	123	5	mhz	mhz	NOUN
eurjchem-1477	123	6	,	,	PUNCT
eurjchem-1477	123	7	cdcl3	cdcl3	PROPN
eurjchem-1477	123	8	,	,	PUNCT
eurjchem-1477	123	9	δ	δ	PROPN
eurjchem-1477	123	10	,	,	PUNCT
eurjchem-1477	123	11	ppm	ppm	NOUN
eurjchem-1477	123	12	):	):	PUNCT
eurjchem-1477	123	13	3.24	3.24	NUM
eurjchem-1477	123	14	(	(	PUNCT
eurjchem-1477	123	15	s	s	PROPN
eurjchem-1477	123	16	,	,	PUNCT
eurjchem-1477	123	17	2h	2h	NUM
eurjchem-1477	123	18	,	,	PUNCT
eurjchem-1477	123	19	azepine‐ch2	azepine‐ch2	NUM
eurjchem-1477	123	20	)	)	PUNCT
eurjchem-1477	123	21	,	,	PUNCT
eurjchem-1477	123	22	6.30‐6.31	6.30‐6.31	PROPN
eurjchem-1477	123	23	(	(	PUNCT
eurjchem-1477	123	24	d	d	PROPN
eurjchem-1477	123	25	,	,	PUNCT
eurjchem-1477	123	26	1h	1h	NUM
eurjchem-1477	123	27	,	,	PUNCT
eurjchem-1477	123	28	j	j	PROPN
eurjchem-1477	123	29	=	=	SYM
eurjchem-1477	123	30	4.4	4.4	NUM
eurjchem-1477	123	31	hz	hz	VERB
eurjchem-1477	123	32	,	,	PUNCT
eurjchem-1477	123	33	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	123	34	)	)	PUNCT
eurjchem-1477	123	35	,	,	PUNCT
eurjchem-1477	123	36	7.29‐7.20	7.29‐7.20	NUM
eurjchem-1477	123	37	(	(	PUNCT
eurjchem-1477	123	38	d	d	PROPN
eurjchem-1477	123	39	,	,	PUNCT
eurjchem-1477	123	40	1h	1h	NUM
eurjchem-1477	123	41	,	,	PUNCT
eurjchem-1477	123	42	j	j	PROPN
eurjchem-1477	123	43	=	=	SYM
eurjchem-1477	123	44	4.4	4.4	NUM
eurjchem-1477	123	45	hz	hz	NOUN
eurjchem-1477	123	46	,	,	PUNCT
eurjchem-1477	123	47	ar‐	ar‐	PROPN
eurjchem-1477	123	48	h	h	NOUN
eurjchem-1477	123	49	)	)	PUNCT
eurjchem-1477	123	50	,	,	PUNCT
eurjchem-1477	123	51	7.33‐7.35	7.33‐7.35	NUM
eurjchem-1477	123	52	(	(	PUNCT
eurjchem-1477	123	53	d	d	PROPN
eurjchem-1477	123	54	,	,	PUNCT
eurjchem-1477	123	55	1h	1h	NUM
eurjchem-1477	123	56	,	,	PUNCT
eurjchem-1477	123	57	j	j	PROPN
eurjchem-1477	123	58	=	=	PROPN
eurjchem-1477	123	59	8.4	8.4	NUM
eurjchem-1477	123	60	hz	hz	NOUN
eurjchem-1477	123	61	,	,	PUNCT
eurjchem-1477	123	62	ar‐h	ar‐h	PROPN
eurjchem-1477	123	63	)	)	PUNCT
eurjchem-1477	123	64	,	,	PUNCT
eurjchem-1477	123	65	7.71	7.71	NUM
eurjchem-1477	123	66	(	(	PUNCT
eurjchem-1477	123	67	s	s	PROPN
eurjchem-1477	123	68	,	,	PUNCT
eurjchem-1477	123	69	1h	1h	NUM
eurjchem-1477	123	70	,	,	PUNCT
eurjchem-1477	123	71	ar‐h	ar‐h	NOUN
eurjchem-1477	123	72	)	)	PUNCT
eurjchem-1477	123	73	,	,	PUNCT
eurjchem-1477	123	74	7.92‐	7.92‐	NUM
eurjchem-1477	123	75	7.94	7.94	NUM
eurjchem-1477	123	76	(	(	PUNCT
eurjchem-1477	123	77	d	d	PROPN
eurjchem-1477	123	78	,	,	PUNCT
eurjchem-1477	123	79	1h	1h	NUM
eurjchem-1477	123	80	,	,	PUNCT
eurjchem-1477	123	81	j	j	PROPN
eurjchem-1477	123	82	=	=	SYM
eurjchem-1477	123	83	8.0	8.0	NUM
eurjchem-1477	123	84	hz	hz	NOUN
eurjchem-1477	123	85	,	,	PUNCT
eurjchem-1477	123	86	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	123	87	)	)	PUNCT
eurjchem-1477	123	88	,	,	PUNCT
eurjchem-1477	123	89	9.44	9.44	NUM
eurjchem-1477	123	90	(	(	PUNCT
eurjchem-1477	123	91	s	s	PROPN
eurjchem-1477	123	92	,	,	PUNCT
eurjchem-1477	123	93	1h	1h	NUM
eurjchem-1477	123	94	,	,	PUNCT
eurjchem-1477	123	95	nh	nh	PROPN
eurjchem-1477	123	96	)	)	PUNCT
eurjchem-1477	123	97	.	.	PUNCT
eurjchem-1477	124	1	13c	13c	NOUN
eurjchem-1477	124	2	nmr	nmr	NOUN
eurjchem-1477	124	3	(	(	PUNCT
eurjchem-1477	124	4	100	100	NUM
eurjchem-1477	124	5	mhz	mhz	NOUN
eurjchem-1477	124	6	,	,	PUNCT
eurjchem-1477	124	7	cdcl3	cdcl3	PROPN
eurjchem-1477	124	8	,	,	PUNCT
eurjchem-1477	124	9	δ	δ	PROPN
eurjchem-1477	124	10	,	,	PUNCT
eurjchem-1477	124	11	ppm	ppm	NUM
eurjchem-1477	124	12	):	):	PUNCT
eurjchem-1477	124	13	169.28	169.28	NUM
eurjchem-1477	124	14	(	(	PUNCT
eurjchem-1477	124	15	1c	1c	NOUN
eurjchem-1477	124	16	,	,	PUNCT
eurjchem-1477	124	17	ar‐c	ar‐c	PROPN
eurjchem-1477	124	18	)	)	PUNCT
eurjchem-1477	124	19	,	,	PUNCT
eurjchem-1477	124	20	160.44	160.44	NUM
eurjchem-1477	124	21	(	(	PUNCT
eurjchem-1477	124	22	1c	1c	NOUN
eurjchem-1477	124	23	,	,	PUNCT
eurjchem-1477	124	24	ar‐c	ar‐c	PROPN
eurjchem-1477	124	25	)	)	PUNCT
eurjchem-1477	124	26	,	,	PUNCT
eurjchem-1477	124	27	132.56	132.56	NUM
eurjchem-1477	124	28	(	(	PUNCT
eurjchem-1477	124	29	1c	1c	NUM
eurjchem-1477	124	30	,	,	PUNCT
eurjchem-1477	124	31	ar‐c	ar‐c	PROPN
eurjchem-1477	124	32	)	)	PUNCT
eurjchem-1477	124	33	,	,	PUNCT
eurjchem-1477	124	34	128.84	128.84	NUM
eurjchem-1477	124	35	(	(	PUNCT
eurjchem-1477	124	36	1c	1c	NUM
eurjchem-1477	124	37	,	,	PUNCT
eurjchem-1477	124	38	ar‐c	ar‐c	PROPN
eurjchem-1477	124	39	)	)	PUNCT
eurjchem-1477	124	40	,	,	PUNCT
eurjchem-1477	124	41	127.33	127.33	NUM
eurjchem-1477	124	42	(	(	PUNCT
eurjchem-1477	124	43	1c	1c	NOUN
eurjchem-1477	124	44	,	,	PUNCT
eurjchem-1477	124	45	ar‐c	ar‐c	PROPN
eurjchem-1477	124	46	)	)	PUNCT
eurjchem-1477	124	47	,	,	PUNCT
eurjchem-1477	124	48	122.78	122.78	NUM
eurjchem-1477	124	49	(	(	PUNCT
eurjchem-1477	124	50	1c	1c	NUM
eurjchem-1477	124	51	,	,	PUNCT
eurjchem-1477	124	52	ar‐c	ar‐c	PROPN
eurjchem-1477	124	53	)	)	PUNCT
eurjchem-1477	124	54	,	,	PUNCT
eurjchem-1477	124	55	116.65	116.65	NUM
eurjchem-1477	124	56	(	(	PUNCT
eurjchem-1477	124	57	1c	1c	NOUN
eurjchem-1477	124	58	,	,	PUNCT
eurjchem-1477	124	59	ar‐c	ar‐c	PROPN
eurjchem-1477	124	60	)	)	PUNCT
eurjchem-1477	124	61	,	,	PUNCT
eurjchem-1477	124	62	113.98	113.98	NUM
eurjchem-1477	124	63	(	(	PUNCT
eurjchem-1477	124	64	1c	1c	NOUN
eurjchem-1477	124	65	,	,	PUNCT
eurjchem-1477	124	66	chnh	chnh	NOUN
eurjchem-1477	124	67	)	)	PUNCT
eurjchem-1477	124	68	,	,	PUNCT
eurjchem-1477	124	69	113.41	113.41	NUM
eurjchem-1477	124	70	(	(	PUNCT
eurjchem-1477	124	71	1c	1c	NOUN
eurjchem-1477	124	72	,	,	PUNCT
eurjchem-1477	124	73	ch‐chnh	ch‐chnh	PROPN
eurjchem-1477	124	74	)	)	PUNCT
eurjchem-1477	124	75	,	,	PUNCT
eurjchem-1477	124	76	43.66	43.66	NUM
eurjchem-1477	124	77	(	(	PUNCT
eurjchem-1477	124	78	1c	1c	NOUN
eurjchem-1477	124	79	,	,	PUNCT
eurjchem-1477	124	80	ch2‐conh	ch2‐conh	NOUN
eurjchem-1477	124	81	)	)	PUNCT
eurjchem-1477	124	82	.	.	PUNCT
eurjchem-1477	125	1	ms	ms	NOUN
eurjchem-1477	125	2	(	(	PUNCT
eurjchem-1477	125	3	ei	ei	PROPN
eurjchem-1477	125	4	,	,	PUNCT
eurjchem-1477	125	5	m	m	PROPN
eurjchem-1477	125	6	/	/	SYM
eurjchem-1477	125	7	z	z	NOUN
eurjchem-1477	125	8	):	):	PUNCT
eurjchem-1477	125	9	239.0896	239.0896	NUM
eurjchem-1477	125	10	(	(	PUNCT
eurjchem-1477	125	11	m+1	m+1	NUM
eurjchem-1477	125	12	)	)	PUNCT
eurjchem-1477	125	13	.	.	PUNCT
eurjchem-1477	126	1	anal	anal	PROPN
eurjchem-1477	126	2	.	.	PUNCT
eurjchem-1477	126	3	calcd	calcd	NOUN
eurjchem-1477	126	4	.	.	PUNCT
eurjchem-1477	127	1	for	for	ADP
eurjchem-1477	127	2	c10h8brno	c10h8brno	PROPN
eurjchem-1477	127	3	:	:	PUNCT
eurjchem-1477	127	4	c	c	X
eurjchem-1477	127	5	,	,	PUNCT
eurjchem-1477	127	6	50.45	50.45	NUM
eurjchem-1477	127	7	;	;	PUNCT
eurjchem-1477	127	8	h	h	X
eurjchem-1477	127	9	,	,	PUNCT
eurjchem-1477	127	10	3.39	3.39	NUM
eurjchem-1477	127	11	;	;	PUNCT
eurjchem-1477	127	12	n	n	CCONJ
eurjchem-1477	127	13	,	,	PUNCT
eurjchem-1477	127	14	5.88	5.88	NUM
eurjchem-1477	127	15	;	;	PUNCT
eurjchem-1477	127	16	o	o	NOUN
eurjchem-1477	127	17	,	,	PUNCT
eurjchem-1477	127	18	6.72	6.72	NUM
eurjchem-1477	127	19	.	.	PUNCT
eurjchem-1477	127	20	found	find	VERB
eurjchem-1477	127	21	:	:	PUNCT
eurjchem-1477	128	1	c	c	X
eurjchem-1477	128	2	,	,	PUNCT
eurjchem-1477	128	3	50.47	50.47	NUM
eurjchem-1477	128	4	;	;	PUNCT
eurjchem-1477	128	5	h	h	NOUN
eurjchem-1477	128	6	,	,	PUNCT
eurjchem-1477	128	7	3.37	3.37	NUM
eurjchem-1477	128	8	;	;	PUNCT
eurjchem-1477	128	9	n	n	CCONJ
eurjchem-1477	128	10	,	,	PUNCT
eurjchem-1477	128	11	5.87	5.87	NUM
eurjchem-1477	128	12	;	;	PUNCT
eurjchem-1477	128	13	o	o	NOUN
eurjchem-1477	128	14	,	,	PUNCT
eurjchem-1477	128	15	6.70	6.70	NUM
eurjchem-1477	128	16	%	%	NOUN
eurjchem-1477	128	17	.	.	PUNCT
eurjchem-1477	129	1	7	7	NUM
eurjchem-1477	129	2	,	,	PUNCT
eurjchem-1477	129	3	8‐dichloro‐1	8‐dichloro‐1	NUM
eurjchem-1477	129	4	,	,	PUNCT
eurjchem-1477	129	5	3‐dihydro‐benzo[d]azepin‐2‐one	3‐dihydro‐benzo[d]azepin‐2‐one	NUM
eurjchem-1477	129	6	(	(	PUNCT
eurjchem-1477	129	7	3h	3h	NUM
eurjchem-1477	129	8	):	):	PUNCT
eurjchem-1477	129	9	color	color	NOUN
eurjchem-1477	129	10	:	:	PUNCT
eurjchem-1477	129	11	light	light	ADJ
eurjchem-1477	129	12	brown	brown	PROPN
eurjchem-1477	129	13	solid	solid	ADJ
eurjchem-1477	129	14	.	.	PUNCT
eurjchem-1477	130	1	yield	yield	NOUN
eurjchem-1477	130	2	:	:	PUNCT
eurjchem-1477	130	3	93	93	NUM
eurjchem-1477	130	4	%	%	NOUN
eurjchem-1477	130	5	.	.	PUNCT
eurjchem-1477	131	1	m.p	m.p	PROPN
eurjchem-1477	131	2	.	.	PROPN
eurjchem-1477	131	3	:	:	PUNCT
eurjchem-1477	132	1	175‐177	175‐177	NUM
eurjchem-1477	132	2	°	°	SYM
eurjchem-1477	132	3	c	c	PROPN
eurjchem-1477	132	4	.	.	PUNCT
eurjchem-1477	133	1	1h	1h	NUM
eurjchem-1477	133	2	nmr	nmr	NOUN
eurjchem-1477	133	3	(	(	PUNCT
eurjchem-1477	133	4	400	400	NUM
eurjchem-1477	133	5	mhz	mhz	NOUN
eurjchem-1477	133	6	,	,	PUNCT
eurjchem-1477	133	7	cdcl3	cdcl3	PROPN
eurjchem-1477	133	8	,	,	PUNCT
eurjchem-1477	133	9	δ	δ	PROPN
eurjchem-1477	133	10	,	,	PUNCT
eurjchem-1477	133	11	ppm	ppm	NOUN
eurjchem-1477	133	12	):	):	PUNCT
eurjchem-1477	133	13	3.24	3.24	NUM
eurjchem-1477	133	14	(	(	PUNCT
eurjchem-1477	133	15	s	s	PROPN
eurjchem-1477	133	16	,	,	PUNCT
eurjchem-1477	133	17	2h	2h	NUM
eurjchem-1477	133	18	,	,	PUNCT
eurjchem-1477	133	19	azepine‐ch2	azepine‐ch2	NUM
eurjchem-1477	133	20	)	)	PUNCT
eurjchem-1477	133	21	,	,	PUNCT
eurjchem-1477	133	22	6.15‐6.13	6.15‐6.13	NUM
eurjchem-1477	133	23	(	(	PUNCT
eurjchem-1477	133	24	d	d	PROPN
eurjchem-1477	133	25	,	,	PUNCT
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eurjchem-1477	133	28	j	j	PROPN
eurjchem-1477	133	29	=	=	SYM
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eurjchem-1477	133	32	,	,	PUNCT
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eurjchem-1477	133	35	,	,	PUNCT
eurjchem-1477	133	36	6.22‐6.20	6.22‐6.20	NUM
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eurjchem-1477	133	38	d	d	PROPN
eurjchem-1477	133	39	,	,	PUNCT
eurjchem-1477	133	40	1h	1h	NUM
eurjchem-1477	133	41	,	,	PUNCT
eurjchem-1477	133	42	j	j	PROPN
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eurjchem-1477	134	3	hz	hz	NOUN
eurjchem-1477	134	4	,	,	PUNCT
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eurjchem-1477	134	7	,	,	PUNCT
eurjchem-1477	134	8	6.85	6.85	NUM
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eurjchem-1477	134	13	,	,	PUNCT
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eurjchem-1477	134	15	)	)	PUNCT
eurjchem-1477	134	16	,	,	PUNCT
eurjchem-1477	134	17	6.82	6.82	NUM
eurjchem-1477	134	18	(	(	PUNCT
eurjchem-1477	134	19	s	s	PROPN
eurjchem-1477	134	20	,	,	PUNCT
eurjchem-1477	134	21	1h	1h	NUM
eurjchem-1477	134	22	,	,	PUNCT
eurjchem-1477	134	23	ar‐h	ar‐h	NOUN
eurjchem-1477	134	24	)	)	PUNCT
eurjchem-1477	134	25	,	,	PUNCT
eurjchem-1477	134	26	9.48	9.48	NUM
eurjchem-1477	134	27	(	(	PUNCT
eurjchem-1477	134	28	s	s	PROPN
eurjchem-1477	134	29	,	,	PUNCT
eurjchem-1477	134	30	1h	1h	NUM
eurjchem-1477	134	31	,	,	PUNCT
eurjchem-1477	134	32	nh	nh	PROPN
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eurjchem-1477	134	34	.	.	PUNCT
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eurjchem-1477	135	2	nmr	nmr	NOUN
eurjchem-1477	135	3	(	(	PUNCT
eurjchem-1477	135	4	100	100	NUM
eurjchem-1477	135	5	mhz	mhz	NOUN
eurjchem-1477	135	6	,	,	PUNCT
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eurjchem-1477	135	8	,	,	PUNCT
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eurjchem-1477	135	10	,	,	PUNCT
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eurjchem-1477	135	12	):	):	PUNCT
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eurjchem-1477	135	15	1c	1c	NOUN
eurjchem-1477	135	16	,	,	PUNCT
eurjchem-1477	135	17	conh	conh	NOUN
eurjchem-1477	135	18	)	)	PUNCT
eurjchem-1477	135	19	,	,	PUNCT
eurjchem-1477	135	20	157.57	157.57	NUM
eurjchem-1477	135	21	(	(	PUNCT
eurjchem-1477	135	22	1c	1c	NOUN
eurjchem-1477	135	23	,	,	PUNCT
eurjchem-1477	135	24	ar‐c	ar‐c	PROPN
eurjchem-1477	135	25	)	)	PUNCT
eurjchem-1477	135	26	,	,	PUNCT
eurjchem-1477	135	27	132.15	132.15	NUM
eurjchem-1477	135	28	(	(	PUNCT
eurjchem-1477	135	29	1c	1c	NUM
eurjchem-1477	135	30	,	,	PUNCT
eurjchem-1477	135	31	ar‐c	ar‐c	PROPN
eurjchem-1477	135	32	)	)	PUNCT
eurjchem-1477	135	33	,	,	PUNCT
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eurjchem-1477	135	35	(	(	PUNCT
eurjchem-1477	135	36	1c	1c	NOUN
eurjchem-1477	135	37	,	,	PUNCT
eurjchem-1477	135	38	ar‐c	ar‐c	PROPN
eurjchem-1477	135	39	)	)	PUNCT
eurjchem-1477	135	40	,	,	PUNCT
eurjchem-1477	135	41	126.11	126.11	NUM
eurjchem-1477	135	42	(	(	PUNCT
eurjchem-1477	135	43	1c	1c	NOUN
eurjchem-1477	135	44	,	,	PUNCT
eurjchem-1477	135	45	ar‐c	ar‐c	PROPN
eurjchem-1477	135	46	)	)	PUNCT
eurjchem-1477	135	47	,	,	PUNCT
eurjchem-1477	135	48	123.22	123.22	NUM
eurjchem-1477	135	49	(	(	PUNCT
eurjchem-1477	135	50	1c	1c	NOUN
eurjchem-1477	135	51	,	,	PUNCT
eurjchem-1477	135	52	ar‐c	ar‐c	PROPN
eurjchem-1477	135	53	)	)	PUNCT
eurjchem-1477	135	54	,	,	PUNCT
eurjchem-1477	135	55	114.89	114.89	NUM
eurjchem-1477	135	56	(	(	PUNCT
eurjchem-1477	135	57	1c	1c	NOUN
eurjchem-1477	135	58	,	,	PUNCT
eurjchem-1477	135	59	ar‐c	ar‐c	PROPN
eurjchem-1477	135	60	)	)	PUNCT
eurjchem-1477	135	61	,	,	PUNCT
eurjchem-1477	135	62	114.42	114.42	NUM
eurjchem-1477	135	63	(	(	PUNCT
eurjchem-1477	135	64	1c	1c	X
eurjchem-1477	135	65	,	,	PUNCT
eurjchem-1477	135	66	chnh	chnh	NOUN
eurjchem-1477	135	67	)	)	PUNCT
eurjchem-1477	135	68	,	,	PUNCT
eurjchem-1477	135	69	114.21	114.21	NUM
eurjchem-1477	135	70	(	(	PUNCT
eurjchem-1477	135	71	1c	1c	NUM
eurjchem-1477	135	72	,	,	PUNCT
eurjchem-1477	135	73	ch‐chnh	ch‐chnh	PROPN
eurjchem-1477	135	74	)	)	PUNCT
eurjchem-1477	135	75	,	,	PUNCT
eurjchem-1477	135	76	43.07	43.07	NUM
eurjchem-1477	135	77	(	(	PUNCT
eurjchem-1477	135	78	1c	1c	NOUN
eurjchem-1477	135	79	,	,	PUNCT
eurjchem-1477	135	80	ch2‐conh	ch2‐conh	NOUN
eurjchem-1477	135	81	)	)	PUNCT
eurjchem-1477	135	82	.	.	PUNCT
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eurjchem-1477	136	2	(	(	PUNCT
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eurjchem-1477	136	4	,	,	PUNCT
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eurjchem-1477	136	8	):	):	PUNCT
eurjchem-1477	136	9	228.0711	228.0711	NUM
eurjchem-1477	136	10	(	(	PUNCT
eurjchem-1477	136	11	m+	m+	NUM
eurjchem-1477	136	12	)	)	PUNCT
eurjchem-1477	136	13	.	.	PUNCT
eurjchem-1477	137	1	anal	anal	PROPN
eurjchem-1477	137	2	.	.	PUNCT
eurjchem-1477	137	3	calcd	calcd	NOUN
eurjchem-1477	137	4	.	.	PUNCT
eurjchem-1477	138	1	for	for	ADP
eurjchem-1477	138	2	c10h7cl2no	c10h7cl2no	NOUN
eurjchem-1477	138	3	:	:	PUNCT
eurjchem-1477	138	4	c	c	NOUN
eurjchem-1477	138	5	,	,	PUNCT
eurjchem-1477	138	6	52.66	52.66	NUM
eurjchem-1477	138	7	;	;	PUNCT
eurjchem-1477	138	8	h	h	NOUN
eurjchem-1477	138	9	,	,	PUNCT
eurjchem-1477	138	10	3.09	3.09	NUM
eurjchem-1477	138	11	;	;	PUNCT
eurjchem-1477	138	12	n	n	CCONJ
eurjchem-1477	138	13	,	,	PUNCT
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eurjchem-1477	138	15	;	;	PUNCT
eurjchem-1477	138	16	o	o	X
eurjchem-1477	138	17	,	,	PUNCT
eurjchem-1477	138	18	7.01	7.01	NUM
eurjchem-1477	138	19	.	.	PUNCT
eurjchem-1477	138	20	found	find	VERB
eurjchem-1477	138	21	:	:	PUNCT
eurjchem-1477	139	1	c	c	X
eurjchem-1477	139	2	,	,	PUNCT
eurjchem-1477	139	3	52.64	52.64	NUM
eurjchem-1477	139	4	;	;	PUNCT
eurjchem-1477	139	5	h	h	NOUN
eurjchem-1477	139	6	,	,	PUNCT
eurjchem-1477	139	7	3.06	3.06	NUM
eurjchem-1477	139	8	;	;	PUNCT
eurjchem-1477	139	9	n	n	CCONJ
eurjchem-1477	139	10	,	,	PUNCT
eurjchem-1477	139	11	6.15	6.15	NUM
eurjchem-1477	139	12	;	;	PUNCT
eurjchem-1477	139	13	o	o	NOUN
eurjchem-1477	139	14	,	,	PUNCT
eurjchem-1477	139	15	7.05	7.05	NUM
eurjchem-1477	139	16	%	%	NOUN
eurjchem-1477	139	17	.	.	PUNCT
eurjchem-1477	140	1	1	1	NUM
eurjchem-1477	140	2	,	,	PUNCT
eurjchem-1477	140	3	3‐dihydro‐1	3‐dihydro‐1	NUM
eurjchem-1477	140	4	,	,	PUNCT
eurjchem-1477	140	5	3‐dihydro‐benzo[d]azepin‐2‐one	3‐dihydro‐benzo[d]azepin‐2‐one	NUM
eurjchem-1477	140	6	(	(	PUNCT
eurjchem-1477	140	7	3i	3i	NUM
eurjchem-1477	140	8	):	):	PUNCT
eurjchem-1477	140	9	color	color	NOUN
eurjchem-1477	140	10	:	:	PUNCT
eurjchem-1477	140	11	light	light	ADJ
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eurjchem-1477	140	13	semisolid	semisolid	NOUN
eurjchem-1477	140	14	.	.	PUNCT
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eurjchem-1477	141	2	:	:	PUNCT
eurjchem-1477	141	3	91	91	NUM
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eurjchem-1477	141	5	.	.	PUNCT
eurjchem-1477	142	1	m.p	m.p	PROPN
eurjchem-1477	142	2	.	.	PROPN
eurjchem-1477	142	3	:	:	PUNCT
eurjchem-1477	143	1	90‐92	90‐92	NUM
eurjchem-1477	144	1	°	°	ADP
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eurjchem-1477	145	1	1h	1h	NUM
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eurjchem-1477	145	3	(	(	PUNCT
eurjchem-1477	145	4	400	400	NUM
eurjchem-1477	145	5	mhz	mhz	NOUN
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eurjchem-1477	145	7	cdcl3	cdcl3	PROPN
eurjchem-1477	145	8	,	,	PUNCT
eurjchem-1477	145	9	δ	δ	PROPN
eurjchem-1477	145	10	,	,	PUNCT
eurjchem-1477	145	11	ppm	ppm	NUM
eurjchem-1477	145	12	):	):	PUNCT
eurjchem-1477	145	13	3.46	3.46	NUM
eurjchem-1477	145	14	(	(	PUNCT
eurjchem-1477	145	15	s	s	PROPN
eurjchem-1477	145	16	,	,	PUNCT
eurjchem-1477	145	17	2h	2h	NUM
eurjchem-1477	145	18	,	,	PUNCT
eurjchem-1477	145	19	azepine‐ch2	azepine‐ch2	NUM
eurjchem-1477	145	20	)	)	PUNCT
eurjchem-1477	145	21	,	,	PUNCT
eurjchem-1477	145	22	6.28‐6.29	6.28‐6.29	X
eurjchem-1477	145	23	(	(	PUNCT
eurjchem-1477	145	24	d	d	PROPN
eurjchem-1477	145	25	,	,	PUNCT
eurjchem-1477	145	26	1h	1h	NUM
eurjchem-1477	145	27	,	,	PUNCT
eurjchem-1477	145	28	j	j	PROPN
eurjchem-1477	145	29	=	=	SYM
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eurjchem-1477	145	31	hz	hz	VERB
eurjchem-1477	145	32	,	,	PUNCT
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eurjchem-1477	145	34	)	)	PUNCT
eurjchem-1477	145	35	,	,	PUNCT
eurjchem-1477	145	36	7.21‐7.22	7.21‐7.22	NUM
eurjchem-1477	145	37	(	(	PUNCT
eurjchem-1477	145	38	d	d	PROPN
eurjchem-1477	145	39	,	,	PUNCT
eurjchem-1477	145	40	1h	1h	NUM
eurjchem-1477	145	41	,	,	PUNCT
eurjchem-1477	145	42	j	j	PROPN
eurjchem-1477	146	1	=	=	SYM
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eurjchem-1477	146	4	,	,	PUNCT
eurjchem-1477	146	5	ar‐	ar‐	PROPN
eurjchem-1477	146	6	h	h	NOUN
eurjchem-1477	146	7	)	)	PUNCT
eurjchem-1477	146	8	,	,	PUNCT
eurjchem-1477	146	9	7.23	7.23	NUM
eurjchem-1477	146	10	(	(	PUNCT
eurjchem-1477	146	11	dd	dd	NOUN
eurjchem-1477	146	12	,	,	PUNCT
eurjchem-1477	146	13	2h	2h	NUM
eurjchem-1477	146	14	,	,	PUNCT
eurjchem-1477	146	15	j	j	PROPN
eurjchem-1477	146	16	=	=	SYM
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eurjchem-1477	146	18	hz	hz	NOUN
eurjchem-1477	146	19	,	,	PUNCT
eurjchem-1477	146	20	ar‐h	ar‐h	NOUN
eurjchem-1477	146	21	)	)	PUNCT
eurjchem-1477	146	22	,	,	PUNCT
eurjchem-1477	146	23	7.38‐7.39	7.38‐7.39	NUM
eurjchem-1477	146	24	(	(	PUNCT
eurjchem-1477	146	25	d	d	PROPN
eurjchem-1477	146	26	,	,	PUNCT
eurjchem-1477	146	27	1h	1h	NUM
eurjchem-1477	146	28	,	,	PUNCT
eurjchem-1477	146	29	j	j	PROPN
eurjchem-1477	146	30	=	=	SYM
eurjchem-1477	146	31	3.6	3.6	NUM
eurjchem-1477	146	32	hz	hz	NOUN
eurjchem-1477	146	33	,	,	PUNCT
eurjchem-1477	146	34	ar‐h	ar‐h	NOUN
eurjchem-1477	146	35	)	)	PUNCT
eurjchem-1477	146	36	,	,	PUNCT
eurjchem-1477	146	37	7.56‐7.58	7.56‐7.58	NUM
eurjchem-1477	146	38	(	(	PUNCT
eurjchem-1477	146	39	d	d	PROPN
eurjchem-1477	146	40	,	,	PUNCT
eurjchem-1477	146	41	1h	1h	NUM
eurjchem-1477	146	42	,	,	PUNCT
eurjchem-1477	146	43	j	j	PROPN
eurjchem-1477	146	44	=	=	PROPN
eurjchem-1477	146	45	8.4	8.4	NUM
eurjchem-1477	146	46	hz	hz	NOUN
eurjchem-1477	146	47	,	,	PUNCT
eurjchem-1477	146	48	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	146	49	)	)	PUNCT
eurjchem-1477	146	50	,	,	PUNCT
eurjchem-1477	146	51	9.43	9.43	NUM
eurjchem-1477	146	52	(	(	PUNCT
eurjchem-1477	146	53	s	s	PROPN
eurjchem-1477	146	54	,	,	PUNCT
eurjchem-1477	146	55	1h	1h	NUM
eurjchem-1477	146	56	,	,	PUNCT
eurjchem-1477	146	57	nh	nh	PROPN
eurjchem-1477	146	58	)	)	PUNCT
eurjchem-1477	146	59	.	.	PUNCT
eurjchem-1477	147	1	13c	13c	NOUN
eurjchem-1477	147	2	nmr	nmr	NOUN
eurjchem-1477	147	3	(	(	PUNCT
eurjchem-1477	147	4	100	100	NUM
eurjchem-1477	147	5	mhz	mhz	NOUN
eurjchem-1477	147	6	,	,	PUNCT
eurjchem-1477	147	7	cdcl3	cdcl3	PROPN
eurjchem-1477	147	8	,	,	PUNCT
eurjchem-1477	147	9	δ	δ	PROPN
eurjchem-1477	147	10	,	,	PUNCT
eurjchem-1477	147	11	ppm	ppm	NUM
eurjchem-1477	147	12	):	):	PUNCT
eurjchem-1477	147	13	169.12	169.12	NUM
eurjchem-1477	147	14	(	(	PUNCT
eurjchem-1477	147	15	1c	1c	NOUN
eurjchem-1477	147	16	,	,	PUNCT
eurjchem-1477	147	17	conh	conh	NOUN
eurjchem-1477	147	18	)	)	PUNCT
eurjchem-1477	147	19	,	,	PUNCT
eurjchem-1477	147	20	159.53	159.53	NUM
eurjchem-1477	147	21	(	(	PUNCT
eurjchem-1477	147	22	1c	1c	NUM
eurjchem-1477	147	23	,	,	PUNCT
eurjchem-1477	147	24	ar‐c	ar‐c	PROPN
eurjchem-1477	147	25	)	)	PUNCT
eurjchem-1477	147	26	,	,	PUNCT
eurjchem-1477	147	27	132.35	132.35	NUM
eurjchem-1477	147	28	(	(	PUNCT
eurjchem-1477	147	29	1c	1c	NOUN
eurjchem-1477	147	30	,	,	PUNCT
eurjchem-1477	147	31	ar‐c	ar‐c	PROPN
eurjchem-1477	147	32	)	)	PUNCT
eurjchem-1477	147	33	,	,	PUNCT
eurjchem-1477	147	34	128.71	128.71	NUM
eurjchem-1477	147	35	(	(	PUNCT
eurjchem-1477	147	36	1c	1c	NOUN
eurjchem-1477	147	37	,	,	PUNCT
eurjchem-1477	147	38	ar‐c	ar‐c	PROPN
eurjchem-1477	147	39	)	)	PUNCT
eurjchem-1477	147	40	,	,	PUNCT
eurjchem-1477	147	41	127.22	127.22	NUM
eurjchem-1477	147	42	(	(	PUNCT
eurjchem-1477	147	43	1c	1c	NUM
eurjchem-1477	147	44	,	,	PUNCT
eurjchem-1477	147	45	ar‐c	ar‐c	PROPN
eurjchem-1477	147	46	)	)	PUNCT
eurjchem-1477	147	47	,	,	PUNCT
eurjchem-1477	147	48	123.14	123.14	NUM
eurjchem-1477	147	49	(	(	PUNCT
eurjchem-1477	147	50	1c	1c	NOUN
eurjchem-1477	147	51	,	,	PUNCT
eurjchem-1477	147	52	ar‐c	ar‐c	PROPN
eurjchem-1477	147	53	)	)	PUNCT
eurjchem-1477	147	54	,	,	PUNCT
eurjchem-1477	147	55	116.31	116.31	NUM
eurjchem-1477	147	56	(	(	PUNCT
eurjchem-1477	147	57	1c	1c	NUM
eurjchem-1477	147	58	,	,	PUNCT
eurjchem-1477	147	59	ar‐c	ar‐c	PROPN
eurjchem-1477	147	60	)	)	PUNCT
eurjchem-1477	147	61	,	,	PUNCT
eurjchem-1477	147	62	113.25	113.25	NUM
eurjchem-1477	147	63	(	(	PUNCT
eurjchem-1477	147	64	1c	1c	NOUN
eurjchem-1477	147	65	,	,	PUNCT
eurjchem-1477	147	66	chnh	chnh	NOUN
eurjchem-1477	147	67	)	)	PUNCT
eurjchem-1477	147	68	,	,	PUNCT
eurjchem-1477	147	69	113.12	113.12	NUM
eurjchem-1477	147	70	(	(	PUNCT
eurjchem-1477	147	71	1c	1c	NOUN
eurjchem-1477	147	72	,	,	PUNCT
eurjchem-1477	147	73	ch‐chnh	ch‐chnh	PROPN
eurjchem-1477	147	74	)	)	PUNCT
eurjchem-1477	147	75	,	,	PUNCT
eurjchem-1477	147	76	41.62	41.62	NUM
eurjchem-1477	147	77	(	(	PUNCT
eurjchem-1477	147	78	1c	1c	NOUN
eurjchem-1477	147	79	,	,	PUNCT
eurjchem-1477	147	80	ch2‐chconh	ch2‐chconh	PROPN
eurjchem-1477	147	81	)	)	PUNCT
eurjchem-1477	147	82	.	.	PUNCT
eurjchem-1477	148	1	ms	ms	NOUN
eurjchem-1477	148	2	(	(	PUNCT
eurjchem-1477	148	3	ei	ei	PROPN
eurjchem-1477	148	4	,	,	PUNCT
eurjchem-1477	148	5	m	m	PROPN
eurjchem-1477	148	6	/	/	SYM
eurjchem-1477	148	7	z	z	PROPN
eurjchem-1477	148	8	):	):	PUNCT
eurjchem-1477	148	9	160.1826	160.1826	NUM
eurjchem-1477	148	10	(	(	PUNCT
eurjchem-1477	148	11	m+1	m+1	NUM
eurjchem-1477	148	12	)	)	PUNCT
eurjchem-1477	148	13	.	.	PUNCT
eurjchem-1477	149	1	anal	anal	PROPN
eurjchem-1477	149	2	.	.	PUNCT
eurjchem-1477	149	3	calcd	calcd	NOUN
eurjchem-1477	149	4	.	.	PUNCT
eurjchem-1477	150	1	for	for	ADP
eurjchem-1477	150	2	c10h9no	c10h9no	NOUN
eurjchem-1477	150	3	:	:	PUNCT
eurjchem-1477	150	4	c	c	X
eurjchem-1477	150	5	,	,	PUNCT
eurjchem-1477	150	6	75.45	75.45	NUM
eurjchem-1477	150	7	;	;	PUNCT
eurjchem-1477	150	8	h	h	NOUN
eurjchem-1477	150	9	,	,	PUNCT
eurjchem-1477	150	10	5.70	5.70	NUM
eurjchem-1477	150	11	;	;	PUNCT
eurjchem-1477	150	12	n	n	CCONJ
eurjchem-1477	150	13	,	,	PUNCT
eurjchem-1477	150	14	8.80	8.80	NUM
eurjchem-1477	150	15	;	;	PUNCT
eurjchem-1477	150	16	o	o	NOUN
eurjchem-1477	150	17	,	,	PUNCT
eurjchem-1477	150	18	10.05	10.05	NUM
eurjchem-1477	150	19	.	.	PUNCT
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eurjchem-1477	150	21	:	:	PUNCT
eurjchem-1477	151	1	c	c	X
eurjchem-1477	151	2	,	,	PUNCT
eurjchem-1477	151	3	75.41	75.41	NUM
eurjchem-1477	151	4	;	;	PUNCT
eurjchem-1477	151	5	h	h	NOUN
eurjchem-1477	151	6	,	,	PUNCT
eurjchem-1477	151	7	5.72	5.72	NUM
eurjchem-1477	151	8	;	;	PUNCT
eurjchem-1477	151	9	n	n	CCONJ
eurjchem-1477	151	10	,	,	PUNCT
eurjchem-1477	151	11	8.83	8.83	NUM
eurjchem-1477	151	12	;	;	PUNCT
eurjchem-1477	151	13	o	o	NOUN
eurjchem-1477	151	14	,	,	PUNCT
eurjchem-1477	151	15	10.02	10.02	NUM
eurjchem-1477	151	16	%	%	NOUN
eurjchem-1477	151	17	.	.	PUNCT
eurjchem-1477	152	1	8‐nitro‐1	8‐nitro‐1	NUM
eurjchem-1477	152	2	,	,	PUNCT
eurjchem-1477	152	3	3‐dihydro‐benzo[d]azepin‐2‐one	3‐dihydro‐benzo[d]azepin‐2‐one	NUM
eurjchem-1477	152	4	(	(	PUNCT
eurjchem-1477	152	5	3j	3j	NUM
eurjchem-1477	152	6	):	):	PUNCT
eurjchem-1477	152	7	color	color	NOUN
eurjchem-1477	152	8	:	:	PUNCT
eurjchem-1477	152	9	light	light	ADJ
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eurjchem-1477	152	11	semi	semi	X
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eurjchem-1477	152	13	.	.	PUNCT
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eurjchem-1477	152	15	:	:	PUNCT
eurjchem-1477	152	16	90	90	NUM
eurjchem-1477	152	17	%	%	NOUN
eurjchem-1477	152	18	.	.	PUNCT
eurjchem-1477	153	1	m.p	m.p	PROPN
eurjchem-1477	153	2	.	.	PROPN
eurjchem-1477	153	3	:	:	PUNCT
eurjchem-1477	154	1	142‐144	142‐144	NUM
eurjchem-1477	154	2	°	°	PROPN
eurjchem-1477	154	3	c	c	NOUN
eurjchem-1477	154	4	.	.	PUNCT
eurjchem-1477	155	1	1h	1h	NUM
eurjchem-1477	155	2	nmr	nmr	NOUN
eurjchem-1477	155	3	(	(	PUNCT
eurjchem-1477	155	4	400	400	NUM
eurjchem-1477	155	5	mhz	mhz	NOUN
eurjchem-1477	155	6	,	,	PUNCT
eurjchem-1477	155	7	cdcl3	cdcl3	PROPN
eurjchem-1477	155	8	,	,	PUNCT
eurjchem-1477	155	9	δ	δ	PROPN
eurjchem-1477	155	10	,	,	PUNCT
eurjchem-1477	155	11	ppm	ppm	NUM
eurjchem-1477	155	12	):	):	PUNCT
eurjchem-1477	155	13	3.33	3.33	NUM
eurjchem-1477	155	14	(	(	PUNCT
eurjchem-1477	155	15	s	s	PROPN
eurjchem-1477	155	16	,	,	PUNCT
eurjchem-1477	155	17	2h	2h	NUM
eurjchem-1477	155	18	,	,	PUNCT
eurjchem-1477	155	19	azepine‐ch2	azepine‐ch2	NUM
eurjchem-1477	155	20	)	)	PUNCT
eurjchem-1477	155	21	,	,	PUNCT
eurjchem-1477	155	22	6.15‐6.13	6.15‐6.13	NUM
eurjchem-1477	155	23	(	(	PUNCT
eurjchem-1477	155	24	d	d	PROPN
eurjchem-1477	155	25	,	,	PUNCT
eurjchem-1477	155	26	1h	1h	NUM
eurjchem-1477	155	27	,	,	PUNCT
eurjchem-1477	155	28	j	j	PROPN
eurjchem-1477	156	1	=	=	PROPN
eurjchem-1477	156	2	8.4	8.4	NUM
eurjchem-1477	156	3	hz	hz	NOUN
eurjchem-1477	156	4	,	,	PUNCT
eurjchem-1477	156	5	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	156	6	)	)	PUNCT
eurjchem-1477	156	7	,	,	PUNCT
eurjchem-1477	156	8	6.23‐6.22	6.23‐6.22	NUM
eurjchem-1477	156	9	(	(	PUNCT
eurjchem-1477	156	10	d	d	PROPN
eurjchem-1477	156	11	,	,	PUNCT
eurjchem-1477	156	12	1h	1h	NUM
eurjchem-1477	156	13	,	,	PUNCT
eurjchem-1477	156	14	j	j	PROPN
eurjchem-1477	156	15	=	=	SYM
eurjchem-1477	156	16	4.4	4.4	NUM
eurjchem-1477	156	17	hz	hz	NOUN
eurjchem-1477	156	18	,	,	PUNCT
eurjchem-1477	156	19	azepine	azepine	PROPN
eurjchem-1477	156	20	ch	ch	PROPN
eurjchem-1477	156	21	)	)	PUNCT
eurjchem-1477	156	22	,	,	PUNCT
eurjchem-1477	156	23	6.65	6.65	NUM
eurjchem-1477	156	24	(	(	PUNCT
eurjchem-1477	156	25	s	s	PROPN
eurjchem-1477	156	26	,	,	PUNCT
eurjchem-1477	156	27	1h	1h	NUM
eurjchem-1477	156	28	,	,	PUNCT
eurjchem-1477	156	29	ar‐h	ar‐h	NOUN
eurjchem-1477	156	30	)	)	PUNCT
eurjchem-1477	156	31	,	,	PUNCT
eurjchem-1477	156	32	7.64‐7.65	7.64‐7.65	NUM
eurjchem-1477	156	33	(	(	PUNCT
eurjchem-1477	156	34	d	d	PROPN
eurjchem-1477	156	35	,	,	PUNCT
eurjchem-1477	156	36	1h	1h	NUM
eurjchem-1477	156	37	,	,	PUNCT
eurjchem-1477	156	38	j	j	PROPN
eurjchem-1477	156	39	=	=	SYM
eurjchem-1477	156	40	3.6	3.6	NUM
eurjchem-1477	156	41	hz	hz	NOUN
eurjchem-1477	156	42	,	,	PUNCT
eurjchem-1477	156	43	ar‐	ar‐	PROPN
eurjchem-1477	156	44	h	h	NOUN
eurjchem-1477	156	45	)	)	PUNCT
eurjchem-1477	156	46	,	,	PUNCT
eurjchem-1477	156	47	7.85‐7.86	7.85‐7.86	NUM
eurjchem-1477	157	1	(	(	PUNCT
eurjchem-1477	157	2	d	d	PROPN
eurjchem-1477	157	3	,	,	PUNCT
eurjchem-1477	157	4	1h	1h	NUM
eurjchem-1477	157	5	,	,	PUNCT
eurjchem-1477	157	6	j	j	PROPN
eurjchem-1477	157	7	=	=	PROPN
eurjchem-1477	157	8	8.8	8.8	NUM
eurjchem-1477	157	9	hz	hz	NOUN
eurjchem-1477	157	10	,	,	PUNCT
eurjchem-1477	157	11	ar‐h	ar‐h	PROPN
eurjchem-1477	157	12	)	)	PUNCT
eurjchem-1477	157	13	,	,	PUNCT
eurjchem-1477	157	14	9.41	9.41	NUM
eurjchem-1477	157	15	(	(	PUNCT
eurjchem-1477	157	16	s	s	PROPN
eurjchem-1477	157	17	,	,	PUNCT
eurjchem-1477	157	18	1h	1h	NUM
eurjchem-1477	157	19	,	,	PUNCT
eurjchem-1477	157	20	nh	nh	PROPN
eurjchem-1477	157	21	)	)	PUNCT
eurjchem-1477	157	22	.	.	PUNCT
eurjchem-1477	158	1	13c	13c	NOUN
eurjchem-1477	158	2	nmr	nmr	NOUN
eurjchem-1477	158	3	(	(	PUNCT
eurjchem-1477	158	4	100	100	NUM
eurjchem-1477	158	5	mhz	mhz	NOUN
eurjchem-1477	158	6	,	,	PUNCT
eurjchem-1477	158	7	cdcl3	cdcl3	PROPN
eurjchem-1477	158	8	,	,	PUNCT
eurjchem-1477	158	9	δ	δ	PROPN
eurjchem-1477	158	10	,	,	PUNCT
eurjchem-1477	158	11	ppm	ppm	NUM
eurjchem-1477	158	12	):	):	PUNCT
eurjchem-1477	158	13	168.31	168.31	NUM
eurjchem-1477	158	14	(	(	PUNCT
eurjchem-1477	158	15	1c	1c	NOUN
eurjchem-1477	158	16	,	,	PUNCT
eurjchem-1477	158	17	conh	conh	NOUN
eurjchem-1477	158	18	)	)	PUNCT
eurjchem-1477	158	19	,	,	PUNCT
eurjchem-1477	158	20	157.34	157.34	NUM
eurjchem-1477	158	21	(	(	PUNCT
eurjchem-1477	158	22	1c	1c	NOUN
eurjchem-1477	158	23	,	,	PUNCT
eurjchem-1477	158	24	ar‐	ar‐	NOUN
eurjchem-1477	158	25	c	c	NOUN
eurjchem-1477	158	26	)	)	PUNCT
eurjchem-1477	158	27	,	,	PUNCT
eurjchem-1477	158	28	132.44	132.44	NUM
eurjchem-1477	158	29	(	(	PUNCT
eurjchem-1477	158	30	1c	1c	NOUN
eurjchem-1477	158	31	,	,	PUNCT
eurjchem-1477	158	32	ar‐c	ar‐c	PROPN
eurjchem-1477	158	33	)	)	PUNCT
eurjchem-1477	158	34	,	,	PUNCT
eurjchem-1477	158	35	128.10	128.10	NUM
eurjchem-1477	158	36	(	(	PUNCT
eurjchem-1477	158	37	1c	1c	NOUN
eurjchem-1477	158	38	,	,	PUNCT
eurjchem-1477	158	39	ar‐c	ar‐c	PROPN
eurjchem-1477	158	40	)	)	PUNCT
eurjchem-1477	158	41	,	,	PUNCT
eurjchem-1477	158	42	125.67	125.67	NUM
eurjchem-1477	158	43	(	(	PUNCT
eurjchem-1477	158	44	1c	1c	NOUN
eurjchem-1477	158	45	,	,	PUNCT
eurjchem-1477	158	46	ar‐c	ar‐c	PROPN
eurjchem-1477	158	47	)	)	PUNCT
eurjchem-1477	158	48	,	,	PUNCT
eurjchem-1477	158	49	123.18	123.18	NUM
eurjchem-1477	158	50	(	(	PUNCT
eurjchem-1477	158	51	1c	1c	NUM
eurjchem-1477	158	52	,	,	PUNCT
eurjchem-1477	158	53	ar‐c	ar‐c	PROPN
eurjchem-1477	158	54	)	)	PUNCT
eurjchem-1477	158	55	,	,	PUNCT
eurjchem-1477	158	56	114.35	114.35	NUM
eurjchem-1477	158	57	(	(	PUNCT
eurjchem-1477	158	58	1c	1c	NOUN
eurjchem-1477	158	59	,	,	PUNCT
eurjchem-1477	158	60	ar‐c	ar‐c	PROPN
eurjchem-1477	158	61	)	)	PUNCT
eurjchem-1477	158	62	,	,	PUNCT
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eurjchem-1477	158	64	(	(	PUNCT
eurjchem-1477	158	65	1c	1c	NOUN
eurjchem-1477	158	66	,	,	PUNCT
eurjchem-1477	158	67	chnh	chnh	NOUN
eurjchem-1477	158	68	)	)	PUNCT
eurjchem-1477	158	69	,	,	PUNCT
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eurjchem-1477	158	71	(	(	PUNCT
eurjchem-1477	158	72	1c	1c	NOUN
eurjchem-1477	158	73	,	,	PUNCT
eurjchem-1477	158	74	ch‐chnh	ch‐chnh	PROPN
eurjchem-1477	158	75	)	)	PUNCT
eurjchem-1477	158	76	,	,	PUNCT
eurjchem-1477	158	77	43.17(1c	43.17(1c	NOUN
eurjchem-1477	158	78	,	,	PUNCT
eurjchem-1477	158	79	ch2‐conh	ch2‐conh	PROPN
eurjchem-1477	158	80	)	)	PUNCT
eurjchem-1477	158	81	.	.	PUNCT
eurjchem-1477	159	1	ms	ms	NOUN
eurjchem-1477	159	2	(	(	PUNCT
eurjchem-1477	159	3	ei	ei	PROPN
eurjchem-1477	159	4	,	,	PUNCT
eurjchem-1477	159	5	m	m	PROPN
eurjchem-1477	159	6	/	/	SYM
eurjchem-1477	159	7	z	z	NOUN
eurjchem-1477	159	8	):	):	PUNCT
eurjchem-1477	159	9	205.1827	205.1827	NUM
eurjchem-1477	159	10	(	(	PUNCT
eurjchem-1477	159	11	m+1	m+1	NUM
eurjchem-1477	159	12	)	)	PUNCT
eurjchem-1477	159	13	.	.	PUNCT
eurjchem-1477	160	1	anal	anal	PROPN
eurjchem-1477	160	2	.	.	PUNCT
eurjchem-1477	160	3	calcd	calcd	NOUN
eurjchem-1477	160	4	.	.	PUNCT
eurjchem-1477	161	1	for	for	ADP
eurjchem-1477	161	2	c10h8n2o3	c10h8n2o3	NOUN
eurjchem-1477	161	3	:	:	PUNCT
eurjchem-1477	161	4	c	c	X
eurjchem-1477	161	5	,	,	PUNCT
eurjchem-1477	161	6	58.82	58.82	NUM
eurjchem-1477	161	7	;	;	PUNCT
eurjchem-1477	161	8	h	h	NOUN
eurjchem-1477	161	9	,	,	PUNCT
eurjchem-1477	161	10	3.95	3.95	NUM
eurjchem-1477	161	11	;	;	PUNCT
eurjchem-1477	161	12	n	n	CCONJ
eurjchem-1477	161	13	,	,	PUNCT
eurjchem-1477	161	14	13.72	13.72	NUM
eurjchem-1477	161	15	;	;	PUNCT
eurjchem-1477	161	16	o	o	NOUN
eurjchem-1477	161	17	,	,	PUNCT
eurjchem-1477	161	18	23.51	23.51	NUM
eurjchem-1477	161	19	.	.	PUNCT
eurjchem-1477	162	1	found	find	VERB
eurjchem-1477	162	2	:	:	PUNCT
eurjchem-1477	163	1	c	c	X
eurjchem-1477	163	2	,	,	PUNCT
eurjchem-1477	163	3	58.81	58.81	NUM
eurjchem-1477	163	4	;	;	PUNCT
eurjchem-1477	163	5	h	h	NOUN
eurjchem-1477	163	6	,	,	PUNCT
eurjchem-1477	163	7	3.98	3.98	NUM
eurjchem-1477	163	8	;	;	PUNCT
eurjchem-1477	163	9	n	n	CCONJ
eurjchem-1477	163	10	,	,	PUNCT
eurjchem-1477	163	11	13.70	13.70	NUM
eurjchem-1477	163	12	;	;	PUNCT
eurjchem-1477	163	13	o	o	NOUN
eurjchem-1477	163	14	,	,	PUNCT
eurjchem-1477	163	15	23.54	23.54	NUM
eurjchem-1477	163	16	%	%	NOUN
eurjchem-1477	163	17	.	.	PUNCT
eurjchem-1477	164	1	7	7	NUM
eurjchem-1477	164	2	,	,	PUNCT
eurjchem-1477	164	3	8‐dimethoxy‐1	8‐dimethoxy‐1	NUM
eurjchem-1477	164	4	,	,	PUNCT
eurjchem-1477	164	5	3‐dihydro‐benzo[d]azepin‐2‐one	3‐dihydro‐benzo[d]azepin‐2‐one	NUM
eurjchem-1477	164	6	(	(	PUNCT
eurjchem-1477	164	7	3k	3k	NUM
eurjchem-1477	164	8	):	):	PUNCT
eurjchem-1477	164	9	color	color	NOUN
eurjchem-1477	164	10	:	:	PUNCT
eurjchem-1477	164	11	light	light	ADJ
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eurjchem-1477	164	14	.	.	PUNCT
eurjchem-1477	165	1	yield	yield	NOUN
eurjchem-1477	165	2	:	:	PUNCT
eurjchem-1477	165	3	85	85	NUM
eurjchem-1477	165	4	%	%	NOUN
eurjchem-1477	165	5	.	.	PUNCT
eurjchem-1477	166	1	m.p	m.p	PROPN
eurjchem-1477	166	2	.	.	PROPN
eurjchem-1477	166	3	:	:	PUNCT
eurjchem-1477	167	1	146‐147	146‐147	NUM
eurjchem-1477	167	2	°	°	PROPN
eurjchem-1477	167	3	c	c	PROPN
eurjchem-1477	167	4	.	.	PUNCT
eurjchem-1477	168	1	1h	1h	NUM
eurjchem-1477	168	2	nmr	nmr	NOUN
eurjchem-1477	168	3	(	(	PUNCT
eurjchem-1477	168	4	400	400	NUM
eurjchem-1477	168	5	mhz	mhz	NOUN
eurjchem-1477	168	6	,	,	PUNCT
eurjchem-1477	168	7	cdcl3	cdcl3	PROPN
eurjchem-1477	168	8	,	,	PUNCT
eurjchem-1477	168	9	δ	δ	PROPN
eurjchem-1477	168	10	,	,	PUNCT
eurjchem-1477	168	11	ppm	ppm	NUM
eurjchem-1477	168	12	):	):	PUNCT
eurjchem-1477	168	13	3.25	3.25	NUM
eurjchem-1477	168	14	(	(	PUNCT
eurjchem-1477	168	15	s	s	PROPN
eurjchem-1477	168	16	,	,	PUNCT
eurjchem-1477	168	17	2h	2h	NUM
eurjchem-1477	168	18	,	,	PUNCT
eurjchem-1477	168	19	azepine‐ch2	azepine‐ch2	NUM
eurjchem-1477	168	20	)	)	PUNCT
eurjchem-1477	168	21	,	,	PUNCT
eurjchem-1477	168	22	3.69	3.69	NUM
eurjchem-1477	168	23	(	(	PUNCT
eurjchem-1477	168	24	s	s	PROPN
eurjchem-1477	168	25	,	,	PUNCT
eurjchem-1477	168	26	6h	6h	NUM
eurjchem-1477	168	27	,	,	PUNCT
eurjchem-1477	168	28	och3	och3	ADJ
eurjchem-1477	168	29	)	)	PUNCT
eurjchem-1477	168	30	,	,	PUNCT
eurjchem-1477	168	31	6.15‐6.13	6.15‐6.13	NUM
eurjchem-1477	168	32	(	(	PUNCT
eurjchem-1477	168	33	d	d	PROPN
eurjchem-1477	168	34	,	,	PUNCT
eurjchem-1477	168	35	1h	1h	NUM
eurjchem-1477	168	36	,	,	PUNCT
eurjchem-1477	168	37	j	j	PROPN
eurjchem-1477	168	38	=	=	SYM
eurjchem-1477	168	39	4.8	4.8	NUM
eurjchem-1477	168	40	hz	hz	VERB
eurjchem-1477	168	41	,	,	PUNCT
eurjchem-1477	168	42	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	168	43	)	)	PUNCT
eurjchem-1477	168	44	,	,	PUNCT
eurjchem-1477	168	45	6.22‐6.20	6.22‐6.20	NUM
eurjchem-1477	168	46	(	(	PUNCT
eurjchem-1477	168	47	d	d	PROPN
eurjchem-1477	168	48	,	,	PUNCT
eurjchem-1477	168	49	1h	1h	NUM
eurjchem-1477	168	50	,	,	PUNCT
eurjchem-1477	168	51	j	j	PROPN
eurjchem-1477	169	1	=	=	PROPN
eurjchem-1477	169	2	8.8	8.8	NUM
eurjchem-1477	169	3	hz	hz	NOUN
eurjchem-1477	169	4	,	,	PUNCT
eurjchem-1477	169	5	azepine‐ch	azepine‐ch	PROPN
eurjchem-1477	169	6	)	)	PUNCT
eurjchem-1477	169	7	,	,	PUNCT
eurjchem-1477	169	8	6.82	6.82	NUM
eurjchem-1477	169	9	(	(	PUNCT
eurjchem-1477	169	10	s	s	PROPN
eurjchem-1477	169	11	,	,	PUNCT
eurjchem-1477	169	12	1h	1h	NUM
eurjchem-1477	169	13	,	,	PUNCT
eurjchem-1477	169	14	ar‐h	ar‐h	NOUN
eurjchem-1477	169	15	)	)	PUNCT
eurjchem-1477	169	16	,	,	PUNCT
eurjchem-1477	169	17	6.85	6.85	NUM
eurjchem-1477	169	18	(	(	PUNCT
eurjchem-1477	169	19	s	s	PROPN
eurjchem-1477	169	20	,	,	PUNCT
eurjchem-1477	169	21	1h	1h	NUM
eurjchem-1477	169	22	,	,	PUNCT
eurjchem-1477	169	23	ar‐h	ar‐h	NOUN
eurjchem-1477	169	24	)	)	PUNCT
eurjchem-1477	169	25	,	,	PUNCT
eurjchem-1477	169	26	9.45	9.45	NUM
eurjchem-1477	169	27	(	(	PUNCT
eurjchem-1477	169	28	s	s	PROPN
eurjchem-1477	169	29	,	,	PUNCT
eurjchem-1477	169	30	1h	1h	NUM
eurjchem-1477	169	31	,	,	PUNCT
eurjchem-1477	169	32	nh	nh	PROPN
eurjchem-1477	169	33	)	)	PUNCT
eurjchem-1477	169	34	.	.	PUNCT
eurjchem-1477	170	1	13c	13c	NOUN
eurjchem-1477	170	2	nmr	nmr	NOUN
eurjchem-1477	170	3	(	(	PUNCT
eurjchem-1477	170	4	100	100	NUM
eurjchem-1477	170	5	mhz	mhz	NOUN
eurjchem-1477	170	6	,	,	PUNCT
eurjchem-1477	170	7	cdcl3	cdcl3	PROPN
eurjchem-1477	170	8	,	,	PUNCT
eurjchem-1477	170	9	δ	δ	PROPN
eurjchem-1477	170	10	,	,	PUNCT
eurjchem-1477	170	11	ppm	ppm	NOUN
eurjchem-1477	170	12	):	):	PUNCT
eurjchem-1477	170	13	169.11	169.11	NUM
eurjchem-1477	170	14	(	(	PUNCT
eurjchem-1477	170	15	1c	1c	X
eurjchem-1477	170	16	,	,	PUNCT
eurjchem-1477	170	17	conh	conh	NOUN
eurjchem-1477	170	18	)	)	PUNCT
eurjchem-1477	170	19	,	,	PUNCT
eurjchem-1477	170	20	149.59	149.59	NUM
eurjchem-1477	170	21	(	(	PUNCT
eurjchem-1477	170	22	1c	1c	NUM
eurjchem-1477	170	23	,	,	PUNCT
eurjchem-1477	170	24	ar‐c	ar‐c	PROPN
eurjchem-1477	170	25	)	)	PUNCT
eurjchem-1477	170	26	,	,	PUNCT
eurjchem-1477	170	27	148.08	148.08	NUM
eurjchem-1477	170	28	(	(	PUNCT
eurjchem-1477	170	29	1c	1c	NOUN
eurjchem-1477	170	30	,	,	PUNCT
eurjchem-1477	170	31	ar‐c	ar‐c	PROPN
eurjchem-1477	170	32	)	)	PUNCT
eurjchem-1477	170	33	,	,	PUNCT
eurjchem-1477	170	34	127.65	127.65	NUM
eurjchem-1477	170	35	(	(	PUNCT
eurjchem-1477	170	36	1c	1c	NOUN
eurjchem-1477	170	37	,	,	PUNCT
eurjchem-1477	170	38	ar‐c	ar‐c	PROPN
eurjchem-1477	170	39	)	)	PUNCT
eurjchem-1477	170	40	,	,	PUNCT
eurjchem-1477	170	41	124.68	124.68	NUM
eurjchem-1477	170	42	(	(	PUNCT
eurjchem-1477	170	43	1c	1c	X
eurjchem-1477	170	44	,	,	PUNCT
eurjchem-1477	170	45	ar‐c	ar‐c	PROPN
eurjchem-1477	170	46	)	)	PUNCT
eurjchem-1477	170	47	,	,	PUNCT
eurjchem-1477	170	48	123.84	123.84	NUM
eurjchem-1477	170	49	(	(	PUNCT
eurjchem-1477	170	50	1c	1c	NOUN
eurjchem-1477	170	51	,	,	PUNCT
eurjchem-1477	170	52	chnh	chnh	NOUN
eurjchem-1477	170	53	)	)	PUNCT
eurjchem-1477	170	54	,	,	PUNCT
eurjchem-1477	170	55	114.78	114.78	NUM
eurjchem-1477	170	56	(	(	PUNCT
eurjchem-1477	170	57	1c	1c	NUM
eurjchem-1477	170	58	,	,	PUNCT
eurjchem-1477	170	59	ar‐c	ar‐c	PROPN
eurjchem-1477	170	60	)	)	PUNCT
eurjchem-1477	170	61	,	,	PUNCT
eurjchem-1477	170	62	112.50	112.50	NUM
eurjchem-1477	170	63	(	(	PUNCT
eurjchem-1477	170	64	1c	1c	NOUN
eurjchem-1477	170	65	,	,	PUNCT
eurjchem-1477	170	66	ar‐c	ar‐c	PROPN
eurjchem-1477	170	67	)	)	PUNCT
eurjchem-1477	170	68	,	,	PUNCT
eurjchem-1477	170	69	110.78	110.78	NUM
eurjchem-1477	170	70	(	(	PUNCT
eurjchem-1477	170	71	1c	1c	NUM
eurjchem-1477	170	72	,	,	PUNCT
eurjchem-1477	170	73	ch‐chnh	ch‐chnh	PROPN
eurjchem-1477	170	74	)	)	PUNCT
eurjchem-1477	170	75	,	,	PUNCT
eurjchem-1477	170	76	56.08	56.08	NUM
eurjchem-1477	170	77	(	(	PUNCT
eurjchem-1477	170	78	2c	2c	NOUN
eurjchem-1477	170	79	,	,	PUNCT
eurjchem-1477	170	80	och3	och3	ADJ
eurjchem-1477	170	81	)	)	PUNCT
eurjchem-1477	170	82	,	,	PUNCT
eurjchem-1477	170	83	43.06	43.06	NUM
eurjchem-1477	170	84	(	(	PUNCT
eurjchem-1477	170	85	1c	1c	NOUN
eurjchem-1477	170	86	,	,	PUNCT
eurjchem-1477	170	87	ch2‐conh	ch2‐conh	NOUN
eurjchem-1477	170	88	)	)	PUNCT
eurjchem-1477	170	89	.	.	PUNCT
eurjchem-1477	171	1	394	394	NUM
eurjchem-1477	171	2	thimmaiah	thimmaiah	NOUN
eurjchem-1477	171	3	et	et	PROPN
eurjchem-1477	171	4	al	al	PROPN
eurjchem-1477	171	5	.	.	PUNCT
eurjchem-1477	171	6	/	/	SYM
eurjchem-1477	171	7	european	european	PROPN
eurjchem-1477	171	8	journal	journal	PROPN
eurjchem-1477	171	9	of	of	ADP
eurjchem-1477	171	10	chemistry	chemistry	NOUN
eurjchem-1477	171	11	7	7	NUM
eurjchem-1477	171	12	(	(	PUNCT
eurjchem-1477	171	13	4	4	NUM
eurjchem-1477	171	14	)	)	PUNCT
eurjchem-1477	171	15	(	(	PUNCT
eurjchem-1477	171	16	2016	2016	NUM
eurjchem-1477	171	17	)	)	PUNCT
eurjchem-1477	171	18	391‐396	391‐396	NUM
eurjchem-1477	171	19	table	table	NOUN
eurjchem-1477	171	20	1	1	NUM
eurjchem-1477	171	21	.	.	PUNCT
eurjchem-1477	171	22	comparison	comparison	NOUN
eurjchem-1477	171	23	of	of	ADP
eurjchem-1477	171	24	reaction	reaction	NOUN
eurjchem-1477	171	25	conditions	condition	NOUN
eurjchem-1477	171	26	and	and	CCONJ
eurjchem-1477	171	27	yield	yield	NOUN
eurjchem-1477	171	28	of	of	ADP
eurjchem-1477	171	29	product	product	NOUN
eurjchem-1477	171	30	with	with	ADP
eurjchem-1477	171	31	reported	report	VERB
eurjchem-1477	171	32	methods	method	NOUN
eurjchem-1477	171	33	with	with	ADP
eurjchem-1477	171	34	the	the	DET
eurjchem-1477	171	35	present	present	ADJ
eurjchem-1477	171	36	method	method	NOUN
eurjchem-1477	171	37	.	.	PUNCT
eurjchem-1477	172	1	entry	entry	NOUN
eurjchem-1477	172	2	methods	method	NOUN
eurjchem-1477	172	3	conditions	condition	NOUN
eurjchem-1477	172	4	time	time	NOUN
eurjchem-1477	172	5	yield	yield	NOUN
eurjchem-1477	172	6	(	(	PUNCT
eurjchem-1477	172	7	%	%	NOUN
eurjchem-1477	172	8	)	)	PUNCT
eurjchem-1477	172	9	reference	reference	NOUN
eurjchem-1477	172	10	1	1	NUM
eurjchem-1477	172	11	pd(pph3)2(oac)2	pd(pph3)2(oac)2	NOUN
eurjchem-1477	172	12	dmf	dmf	PROPN
eurjchem-1477	172	13	,	,	PUNCT
eurjchem-1477	172	14	60	60	NUM
eurjchem-1477	172	15	°	°	NUM
eurjchem-1477	172	16	c	c	NOUN
eurjchem-1477	172	17	16	16	NUM
eurjchem-1477	172	18	hr	hr	NOUN
eurjchem-1477	172	19	80	80	NUM
eurjchem-1477	172	20	15	15	NUM
eurjchem-1477	172	21	2	2	NUM
eurjchem-1477	172	22	conc	conc	NOUN
eurjchem-1477	172	23	.	.	PUNCT
eurjchem-1477	173	1	hcl	hcl	PROPN
eurjchem-1477	173	2	/	/	SYM
eurjchem-1477	173	3	acooh	acooh	PROPN
eurjchem-1477	173	4	dcm	dcm	PROPN
eurjchem-1477	173	5	,	,	PUNCT
eurjchem-1477	173	6	room	room	NOUN
eurjchem-1477	173	7	temp	temp	NOUN
eurjchem-1477	173	8	.	.	PUNCT
eurjchem-1477	174	1	60	60	NUM
eurjchem-1477	174	2	hr	hr	NOUN
eurjchem-1477	174	3	59	59	NUM
eurjchem-1477	174	4	13	13	NUM
eurjchem-1477	174	5	3	3	NUM
eurjchem-1477	174	6	au(pph3)cl	au(pph3)cl	NOUN
eurjchem-1477	174	7	/	/	SYM
eurjchem-1477	174	8	agsbf6	agsbf6	PROPN
eurjchem-1477	174	9	toulene	toulene	NOUN
eurjchem-1477	174	10	,	,	PUNCT
eurjchem-1477	174	11	120	120	NUM
eurjchem-1477	174	12	°	°	NOUN
eurjchem-1477	174	13	c	c	NOUN
eurjchem-1477	174	14	12	12	NUM
eurjchem-1477	174	15	hr	hr	NOUN
eurjchem-1477	174	16	89	89	NUM
eurjchem-1477	174	17	14	14	NUM
eurjchem-1477	174	18	4	4	NUM
eurjchem-1477	174	19	aubr3	aubr3	PROPN
eurjchem-1477	174	20	/	/	SYM
eurjchem-1477	174	21	acooh	acooh	PROPN
eurjchem-1477	174	22	thf	thf	NOUN
eurjchem-1477	174	23	,	,	PUNCT
eurjchem-1477	174	24	120	120	NUM
eurjchem-1477	174	25	°	°	NOUN
eurjchem-1477	174	26	c	c	PROPN
eurjchem-1477	174	27	5	5	NUM
eurjchem-1477	174	28	hr	hr	NOUN
eurjchem-1477	174	29	86	86	NUM
eurjchem-1477	174	30	14	14	NUM
eurjchem-1477	174	31	5	5	NUM
eurjchem-1477	174	32	microwave	microwave	NOUN
eurjchem-1477	174	33	irradiation	irradiation	NOUN
eurjchem-1477	174	34	toulene	toulene	NOUN
eurjchem-1477	174	35	,	,	PUNCT
eurjchem-1477	174	36	120	120	NUM
eurjchem-1477	174	37	°	°	NOUN
eurjchem-1477	174	38	c	c	NOUN
eurjchem-1477	174	39	2‐3	2‐3	NUM
eurjchem-1477	174	40	hr	hr	NOUN
eurjchem-1477	174	41	60	60	NUM
eurjchem-1477	174	42	12	12	NUM
eurjchem-1477	174	43	6	6	NUM
eurjchem-1477	174	44	eaton	eaton	PROPN
eurjchem-1477	174	45	’s	’s	PART
eurjchem-1477	174	46	reagent	reagent	ADJ
eurjchem-1477	174	47	solvent	solvent	NOUN
eurjchem-1477	174	48	free	free	ADJ
eurjchem-1477	174	49	,	,	PUNCT
eurjchem-1477	174	50	room	room	NOUN
eurjchem-1477	174	51	temp	temp	NOUN
eurjchem-1477	174	52	.	.	PUNCT
eurjchem-1477	175	1	10‐15	10‐15	NUM
eurjchem-1477	175	2	min	min	PROPN
eurjchem-1477	175	3	85‐93	85‐93	NUM
eurjchem-1477	175	4	‐	‐	NOUN
eurjchem-1477	175	5	table	table	NOUN
eurjchem-1477	175	6	2	2	NUM
eurjchem-1477	175	7	.	.	PUNCT
eurjchem-1477	175	8	effect	effect	NOUN
eurjchem-1477	175	9	of	of	ADP
eurjchem-1477	175	10	eaton	eaton	PROPN
eurjchem-1477	175	11	’s	’s	PART
eurjchem-1477	175	12	reagent	reagent	ADJ
eurjchem-1477	175	13	concentration	concentration	NOUN
eurjchem-1477	175	14	on	on	ADP
eurjchem-1477	175	15	the	the	DET
eurjchem-1477	175	16	synthesis	synthesis	NOUN
eurjchem-1477	175	17	8‐methoxy‐1,3‐dihydro‐benzo[d]azepin‐2‐one	8‐methoxy‐1,3‐dihydro‐benzo[d]azepin‐2‐one	NUM
eurjchem-1477	175	18	(	(	PUNCT
eurjchem-1477	175	19	3a	3a	NUM
eurjchem-1477	175	20	)	)	PUNCT
eurjchem-1477	175	21	*	*	PUNCT
eurjchem-1477	175	22	.	.	PUNCT
eurjchem-1477	176	1	entry	entry	NOUN
eurjchem-1477	176	2	eaton	eaton	PROPN
eurjchem-1477	176	3	’s	’s	PART
eurjchem-1477	176	4	reagent	reagent	ADJ
eurjchem-1477	176	5	(	(	PUNCT
eurjchem-1477	176	6	mmol	mmol	NOUN
eurjchem-1477	176	7	)	)	PUNCT
eurjchem-1477	176	8	reaction	reaction	NOUN
eurjchem-1477	176	9	time	time	NOUN
eurjchem-1477	176	10	(	(	PUNCT
eurjchem-1477	176	11	min	min	NOUN
eurjchem-1477	176	12	)	)	PUNCT
eurjchem-1477	176	13	yield	yield	NOUN
eurjchem-1477	176	14	(	(	PUNCT
eurjchem-1477	176	15	%	%	NOUN
eurjchem-1477	176	16	)	)	PUNCT
eurjchem-1477	176	17	1	1	NUM
eurjchem-1477	176	18	0.5	0.5	NUM
eurjchem-1477	176	19	10	10	NUM
eurjchem-1477	176	20	80	80	NUM
eurjchem-1477	176	21	2	2	NUM
eurjchem-1477	176	22	1.0	1.0	NUM
eurjchem-1477	176	23	6‐8	6‐8	NUM
eurjchem-1477	176	24	90	90	NUM
eurjchem-1477	176	25	3	3	NUM
eurjchem-1477	176	26	1.5	1.5	NUM
eurjchem-1477	176	27	10‐15	10‐15	NUM
eurjchem-1477	176	28	93	93	NUM
eurjchem-1477	176	29	4	4	NUM
eurjchem-1477	176	30	2.0	2.0	NUM
eurjchem-1477	176	31	10‐14	10‐14	NUM
eurjchem-1477	176	32	92	92	NUM
eurjchem-1477	176	33	5	5	NUM
eurjchem-1477	176	34	2.5	2.5	NUM
eurjchem-1477	176	35	10‐14	10‐14	NUM
eurjchem-1477	176	36	92	92	NUM
eurjchem-1477	176	37	*	*	SYM
eurjchem-1477	176	38	0.39	0.39	NUM
eurjchem-1477	176	39	mmol	mmol	NOUN
eurjchem-1477	176	40	of	of	ADP
eurjchem-1477	176	41	compound	compound	NOUN
eurjchem-1477	176	42	2a	2a	NUM
eurjchem-1477	176	43	.	.	PUNCT
eurjchem-1477	177	1	reaction	reaction	NOUN
eurjchem-1477	177	2	condition	condition	NOUN
eurjchem-1477	177	3	:	:	PUNCT
eurjchem-1477	177	4	room	room	NOUN
eurjchem-1477	177	5	temperature	temperature	NOUN
eurjchem-1477	177	6	,	,	PUNCT
eurjchem-1477	177	7	solvent	solvent	NOUN
eurjchem-1477	177	8	free	free	ADJ
eurjchem-1477	177	9	.	.	PUNCT
eurjchem-1477	178	1	figure	figure	NOUN
eurjchem-1477	178	2	2	2	NUM
eurjchem-1477	178	3	.	.	PUNCT
eurjchem-1477	178	4	proposed	propose	VERB
eurjchem-1477	178	5	mechanism	mechanism	NOUN
eurjchem-1477	178	6	for	for	ADP
eurjchem-1477	178	7	the	the	DET
eurjchem-1477	178	8	synthesis	synthesis	NOUN
eurjchem-1477	178	9	of	of	ADP
eurjchem-1477	178	10	3‐benzazepinones	3‐benzazepinone	NOUN
eurjchem-1477	178	11	.	.	PUNCT
eurjchem-1477	179	1	ms	ms	NOUN
eurjchem-1477	179	2	(	(	PUNCT
eurjchem-1477	179	3	ei	ei	PROPN
eurjchem-1477	179	4	,	,	PUNCT
eurjchem-1477	179	5	m	m	PROPN
eurjchem-1477	179	6	/	/	SYM
eurjchem-1477	179	7	z	z	NOUN
eurjchem-1477	179	8	):	):	PUNCT
eurjchem-1477	179	9	220.2486	220.2486	NUM
eurjchem-1477	179	10	(	(	PUNCT
eurjchem-1477	179	11	m+1	m+1	NUM
eurjchem-1477	179	12	)	)	PUNCT
eurjchem-1477	179	13	.	.	PUNCT
eurjchem-1477	180	1	anal	anal	PROPN
eurjchem-1477	180	2	.	.	PUNCT
eurjchem-1477	180	3	calcd	calcd	NOUN
eurjchem-1477	180	4	.	.	PUNCT
eurjchem-1477	181	1	for	for	ADP
eurjchem-1477	181	2	c12h13no3	c12h13no3	PROPN
eurjchem-1477	181	3	:	:	PUNCT
eurjchem-1477	181	4	c	c	NOUN
eurjchem-1477	181	5	,	,	PUNCT
eurjchem-1477	181	6	65.74	65.74	NUM
eurjchem-1477	181	7	;	;	PUNCT
eurjchem-1477	181	8	h	h	NOUN
eurjchem-1477	181	9	,	,	PUNCT
eurjchem-1477	181	10	5.98	5.98	NUM
eurjchem-1477	181	11	;	;	PUNCT
eurjchem-1477	181	12	n	n	CCONJ
eurjchem-1477	181	13	,	,	PUNCT
eurjchem-1477	181	14	6.39	6.39	NUM
eurjchem-1477	181	15	;	;	PUNCT
eurjchem-1477	181	16	o	o	NOUN
eurjchem-1477	181	17	,	,	PUNCT
eurjchem-1477	181	18	21.89	21.89	NUM
eurjchem-1477	181	19	.	.	PUNCT
eurjchem-1477	181	20	found	find	VERB
eurjchem-1477	181	21	:	:	PUNCT
eurjchem-1477	182	1	c	c	X
eurjchem-1477	182	2	,	,	PUNCT
eurjchem-1477	182	3	65.72	65.72	NUM
eurjchem-1477	182	4	;	;	PUNCT
eurjchem-1477	182	5	h	h	NOUN
eurjchem-1477	182	6	,	,	PUNCT
eurjchem-1477	182	7	5.95	5.95	NUM
eurjchem-1477	182	8	;	;	PUNCT
eurjchem-1477	182	9	n	n	CCONJ
eurjchem-1477	182	10	,	,	PUNCT
eurjchem-1477	182	11	6.33	6.33	NUM
eurjchem-1477	182	12	;	;	PUNCT
eurjchem-1477	182	13	o	o	NOUN
eurjchem-1477	182	14	,	,	PUNCT
eurjchem-1477	182	15	21.92	21.92	NUM
eurjchem-1477	182	16	%	%	NOUN
eurjchem-1477	182	17	.	.	PUNCT
eurjchem-1477	183	1	3	3	X
eurjchem-1477	183	2	.	.	NOUN
eurjchem-1477	183	3	results	result	NOUN
eurjchem-1477	183	4	and	and	CCONJ
eurjchem-1477	183	5	discussion	discussion	NOUN
eurjchem-1477	183	6	for	for	ADP
eurjchem-1477	183	7	every	every	DET
eurjchem-1477	183	8	organic	organic	ADJ
eurjchem-1477	183	9	chemist	chemist	NOUN
eurjchem-1477	183	10	it	it	PRON
eurjchem-1477	183	11	is	be	AUX
eurjchem-1477	183	12	an	an	DET
eurjchem-1477	183	13	unrivalled	unrivalled	ADJ
eurjchem-1477	183	14	dream	dream	NOUN
eurjchem-1477	183	15	to	to	PART
eurjchem-1477	183	16	perform	perform	VERB
eurjchem-1477	183	17	reactions	reaction	NOUN
eurjchem-1477	183	18	under	under	ADP
eurjchem-1477	183	19	solvent	solvent	NOUN
eurjchem-1477	183	20	free	free	ADJ
eurjchem-1477	183	21	and	and	CCONJ
eurjchem-1477	183	22	mild	mild	ADJ
eurjchem-1477	183	23	conditions	condition	NOUN
eurjchem-1477	183	24	for	for	ADP
eurjchem-1477	183	25	providing	provide	VERB
eurjchem-1477	183	26	green	green	ADJ
eurjchem-1477	183	27	approach	approach	NOUN
eurjchem-1477	183	28	towards	towards	ADP
eurjchem-1477	183	29	organic	organic	ADJ
eurjchem-1477	183	30	synthesis	synthesis	NOUN
eurjchem-1477	183	31	.	.	PUNCT
eurjchem-1477	184	1	as	as	ADP
eurjchem-1477	184	2	per	per	ADP
eurjchem-1477	184	3	our	our	PRON
eurjchem-1477	184	4	knowledge	knowledge	NOUN
eurjchem-1477	184	5	here	here	ADV
eurjchem-1477	184	6	in	in	ADP
eurjchem-1477	184	7	,	,	PUNCT
eurjchem-1477	184	8	for	for	ADP
eurjchem-1477	184	9	the	the	DET
eurjchem-1477	184	10	first	first	ADJ
eurjchem-1477	184	11	time	time	NOUN
eurjchem-1477	184	12	we	we	PRON
eurjchem-1477	184	13	are	be	AUX
eurjchem-1477	184	14	reporting	report	VERB
eurjchem-1477	184	15	eaton	eaton	PROPN
eurjchem-1477	184	16	’s	’s	PART
eurjchem-1477	184	17	reagent	reagent	ADJ
eurjchem-1477	184	18	catalysed	catalyse	VERB
eurjchem-1477	184	19	synthesis	synthesis	NOUN
eurjchem-1477	184	20	of	of	ADP
eurjchem-1477	184	21	3‐benzazepinones	3‐benzazepinone	NOUN
eurjchem-1477	184	22	.	.	PUNCT
eurjchem-1477	185	1	we	we	PRON
eurjchem-1477	185	2	found	find	VERB
eurjchem-1477	185	3	that	that	SCONJ
eurjchem-1477	185	4	present	present	ADJ
eurjchem-1477	185	5	method	method	NOUN
eurjchem-1477	185	6	is	be	AUX
eurjchem-1477	185	7	more	more	ADV
eurjchem-1477	185	8	efficient	efficient	ADJ
eurjchem-1477	185	9	compared	compare	VERB
eurjchem-1477	185	10	to	to	ADP
eurjchem-1477	185	11	other	other	ADJ
eurjchem-1477	185	12	reported	report	VERB
eurjchem-1477	185	13	methods	method	NOUN
eurjchem-1477	185	14	(	(	PUNCT
eurjchem-1477	185	15	table	table	NOUN
eurjchem-1477	185	16	1	1	NUM
eurjchem-1477	185	17	)	)	PUNCT
eurjchem-1477	185	18	.	.	PUNCT
eurjchem-1477	186	1	reaction	reaction	NOUN
eurjchem-1477	186	2	protocol	protocol	NOUN
eurjchem-1477	186	3	for	for	ADP
eurjchem-1477	186	4	the	the	DET
eurjchem-1477	186	5	synthesis	synthesis	NOUN
eurjchem-1477	186	6	3‐benzazepinones	3‐benzazepinone	NOUN
eurjchem-1477	186	7	using	use	VERB
eurjchem-1477	186	8	eaton	eaton	PROPN
eurjchem-1477	186	9	’s	’s	PART
eurjchem-1477	186	10	reagent	reagent	NOUN
eurjchem-1477	186	11	is	be	AUX
eurjchem-1477	186	12	as	as	SCONJ
eurjchem-1477	186	13	shown	show	VERB
eurjchem-1477	186	14	in	in	ADP
eurjchem-1477	186	15	scheme	scheme	NOUN
eurjchem-1477	186	16	1	1	NUM
eurjchem-1477	186	17	.	.	PUNCT
eurjchem-1477	187	1	in	in	ADP
eurjchem-1477	187	2	the	the	DET
eurjchem-1477	187	3	beginning	beginning	NOUN
eurjchem-1477	187	4	,	,	PUNCT
eurjchem-1477	187	5	substituted	substitute	VERB
eurjchem-1477	187	6	phenyl	phenyl	NOUN
eurjchem-1477	187	7	acetamide	acetamide	NOUN
eurjchem-1477	187	8	analogues	analogue	NOUN
eurjchem-1477	187	9	were	be	AUX
eurjchem-1477	187	10	synthesized	synthesize	VERB
eurjchem-1477	187	11	from	from	ADP
eurjchem-1477	187	12	different	different	ADJ
eurjchem-1477	187	13	substituted	substitute	VERB
eurjchem-1477	187	14	phenyl	phenyl	NOUN
eurjchem-1477	187	15	acetic	acetic	ADJ
eurjchem-1477	187	16	acids	acid	NOUN
eurjchem-1477	187	17	and	and	CCONJ
eurjchem-1477	187	18	which	which	PRON
eurjchem-1477	187	19	upon	upon	SCONJ
eurjchem-1477	187	20	cyclisation	cyclisation	NOUN
eurjchem-1477	187	21	using	use	VERB
eurjchem-1477	187	22	eaton	eaton	PROPN
eurjchem-1477	187	23	’s	’s	PART
eurjchem-1477	187	24	reagent	reagent	NOUN
eurjchem-1477	187	25	at	at	ADP
eurjchem-1477	187	26	room	room	NOUN
eurjchem-1477	187	27	temperature	temperature	NOUN
eurjchem-1477	187	28	to	to	PART
eurjchem-1477	187	29	get	get	VERB
eurjchem-1477	187	30	3‐benzazepinones	3‐benzazepinones	NUM
eurjchem-1477	187	31	3a‐k	3a‐k	ADJ
eurjchem-1477	187	32	(	(	PUNCT
eurjchem-1477	187	33	table	table	NOUN
eurjchem-1477	187	34	2	2	NUM
eurjchem-1477	187	35	)	)	PUNCT
eurjchem-1477	187	36	.	.	PUNCT
eurjchem-1477	188	1	proposed	propose	VERB
eurjchem-1477	188	2	mechanism	mechanism	NOUN
eurjchem-1477	188	3	for	for	ADP
eurjchem-1477	188	4	the	the	DET
eurjchem-1477	188	5	synthesis	synthesis	NOUN
eurjchem-1477	188	6	of	of	ADP
eurjchem-1477	188	7	3‐benzaze‐	3‐benzaze‐	NUM
eurjchem-1477	188	8	pinones	pinone	NOUN
eurjchem-1477	188	9	is	be	AUX
eurjchem-1477	188	10	as	as	SCONJ
eurjchem-1477	188	11	shown	show	VERB
eurjchem-1477	188	12	in	in	ADP
eurjchem-1477	188	13	figure	figure	NOUN
eurjchem-1477	188	14	2	2	NUM
eurjchem-1477	188	15	.	.	PUNCT
eurjchem-1477	188	16	initially	initially	ADV
eurjchem-1477	188	17	,	,	PUNCT
eurjchem-1477	188	18	n‐dimethoxymethyl‐	n‐dimethoxymethyl‐	ADV
eurjchem-1477	189	1	2‐(3‐methoxy‐phenyl)‐acetamide	2‐(3‐methoxy‐phenyl)‐acetamide	ADJ
eurjchem-1477	189	2	(	(	PUNCT
eurjchem-1477	189	3	2a	2a	NUM
eurjchem-1477	189	4	)	)	PUNCT
eurjchem-1477	189	5	was	be	AUX
eurjchem-1477	189	6	selected	select	VERB
eurjchem-1477	189	7	as	as	ADP
eurjchem-1477	189	8	model	model	NOUN
eurjchem-1477	189	9	substrate	substrate	NOUN
eurjchem-1477	189	10	to	to	PART
eurjchem-1477	189	11	get	get	VERB
eurjchem-1477	189	12	optimal	optimal	ADJ
eurjchem-1477	189	13	reaction	reaction	NOUN
eurjchem-1477	189	14	condition	condition	NOUN
eurjchem-1477	189	15	and	and	CCONJ
eurjchem-1477	189	16	obtained	obtain	VERB
eurjchem-1477	189	17	results	result	NOUN
eurjchem-1477	189	18	are	be	AUX
eurjchem-1477	189	19	tabulated	tabulate	VERB
eurjchem-1477	189	20	in	in	ADP
eurjchem-1477	189	21	table	table	NOUN
eurjchem-1477	189	22	2	2	NUM
eurjchem-1477	189	23	and	and	CCONJ
eurjchem-1477	189	24	3	3	NUM
eurjchem-1477	189	25	.	.	PUNCT
eurjchem-1477	190	1	at	at	ADP
eurjchem-1477	190	2	first	first	ADV
eurjchem-1477	190	3	,	,	PUNCT
eurjchem-1477	190	4	we	we	PRON
eurjchem-1477	190	5	optimized	optimize	VERB
eurjchem-1477	190	6	the	the	DET
eurjchem-1477	190	7	amount	amount	NOUN
eurjchem-1477	190	8	of	of	ADP
eurjchem-1477	190	9	eaton	eaton	PROPN
eurjchem-1477	190	10	’s	’s	PART
eurjchem-1477	190	11	reagent	reagent	NOUN
eurjchem-1477	190	12	required	require	VERB
eurjchem-1477	190	13	for	for	ADP
eurjchem-1477	190	14	the	the	DET
eurjchem-1477	190	15	cyclisation	cyclisation	NOUN
eurjchem-1477	190	16	under	under	ADP
eurjchem-1477	190	17	solvent	solvent	ADJ
eurjchem-1477	190	18	free	free	ADJ
eurjchem-1477	190	19	conditions	condition	NOUN
eurjchem-1477	190	20	and	and	CCONJ
eurjchem-1477	190	21	at	at	ADP
eurjchem-1477	190	22	room	room	NOUN
eurjchem-1477	190	23	temperature	temperature	NOUN
eurjchem-1477	190	24	.	.	PUNCT
eurjchem-1477	191	1	with	with	ADP
eurjchem-1477	191	2	0.5	0.5	NUM
eurjchem-1477	191	3	mmol	mmol	NOUN
eurjchem-1477	191	4	and	and	CCONJ
eurjchem-1477	191	5	1.0	1.0	NUM
eurjchem-1477	191	6	mmol	mmol	NOUN
eurjchem-1477	191	7	of	of	ADP
eurjchem-1477	191	8	eaton	eaton	PROPN
eurjchem-1477	191	9	’s	’s	PART
eurjchem-1477	191	10	reagent	reagent	NOUN
eurjchem-1477	191	11	,	,	PUNCT
eurjchem-1477	191	12	product	product	NOUN
eurjchem-1477	191	13	obtained	obtain	VERB
eurjchem-1477	191	14	in	in	ADP
eurjchem-1477	191	15	moderate	moderate	ADJ
eurjchem-1477	191	16	yield	yield	NOUN
eurjchem-1477	191	17	80	80	NUM
eurjchem-1477	191	18	and	and	CCONJ
eurjchem-1477	191	19	90	90	NUM
eurjchem-1477	191	20	%	%	NOUN
eurjchem-1477	191	21	,	,	PUNCT
eurjchem-1477	191	22	respectively	respectively	ADV
eurjchem-1477	191	23	(	(	PUNCT
eurjchem-1477	191	24	table	table	NOUN
eurjchem-1477	191	25	2	2	NUM
eurjchem-1477	191	26	,	,	PUNCT
eurjchem-1477	191	27	entry	entry	NOUN
eurjchem-1477	191	28	1	1	NUM
eurjchem-1477	191	29	and	and	CCONJ
eurjchem-1477	191	30	2	2	NUM
eurjchem-1477	191	31	)	)	PUNCT
eurjchem-1477	191	32	.	.	PUNCT
eurjchem-1477	192	1	the	the	DET
eurjchem-1477	192	2	better	well	ADJ
eurjchem-1477	192	3	result	result	NOUN
eurjchem-1477	192	4	is	be	AUX
eurjchem-1477	192	5	obtained	obtain	VERB
eurjchem-1477	192	6	when	when	SCONJ
eurjchem-1477	192	7	1.5	1.5	NUM
eurjchem-1477	192	8	mmol	mmol	PROPN
eurjchem-1477	192	9	eaton	eaton	PROPN
eurjchem-1477	192	10	’s	’s	PART
eurjchem-1477	192	11	reagent	reagent	NOUN
eurjchem-1477	192	12	is	be	AUX
eurjchem-1477	192	13	used	use	VERB
eurjchem-1477	192	14	(	(	PUNCT
eurjchem-1477	192	15	table	table	NOUN
eurjchem-1477	192	16	2	2	NUM
eurjchem-1477	192	17	,	,	PUNCT
eurjchem-1477	192	18	entry	entry	NOUN
eurjchem-1477	192	19	3	3	NUM
eurjchem-1477	192	20	,	,	PUNCT
eurjchem-1477	192	21	93	93	NUM
eurjchem-1477	192	22	%	%	NOUN
eurjchem-1477	192	23	)	)	PUNCT
eurjchem-1477	192	24	providing	provide	VERB
eurjchem-1477	192	25	the	the	DET
eurjchem-1477	192	26	desired	desire	VERB
eurjchem-1477	192	27	product	product	NOUN
eurjchem-1477	192	28	in	in	ADP
eurjchem-1477	192	29	excellent	excellent	ADJ
eurjchem-1477	192	30	yield	yield	NOUN
eurjchem-1477	192	31	with	with	ADP
eurjchem-1477	192	32	less	less	ADJ
eurjchem-1477	192	33	reaction	reaction	NOUN
eurjchem-1477	192	34	time	time	NOUN
eurjchem-1477	192	35	,	,	PUNCT
eurjchem-1477	192	36	further	far	ADV
eurjchem-1477	192	37	increasing	increase	VERB
eurjchem-1477	192	38	the	the	DET
eurjchem-1477	192	39	amount	amount	NOUN
eurjchem-1477	192	40	of	of	ADP
eurjchem-1477	192	41	eaton	eaton	PROPN
eurjchem-1477	192	42	’s	’s	PART
eurjchem-1477	192	43	reagent	reagent	NOUN
eurjchem-1477	192	44	did	do	AUX
eurjchem-1477	192	45	not	not	PART
eurjchem-1477	192	46	effect	effect	VERB
eurjchem-1477	192	47	on	on	ADP
eurjchem-1477	192	48	the	the	DET
eurjchem-1477	192	49	yield	yield	NOUN
eurjchem-1477	192	50	or	or	CCONJ
eurjchem-1477	192	51	the	the	DET
eurjchem-1477	192	52	reaction	reaction	NOUN
eurjchem-1477	192	53	time	time	NOUN
eurjchem-1477	192	54	.	.	PUNCT
eurjchem-1477	193	1	therefore	therefore	ADV
eurjchem-1477	193	2	it	it	PRON
eurjchem-1477	193	3	was	be	AUX
eurjchem-1477	193	4	found	find	VERB
eurjchem-1477	193	5	that	that	SCONJ
eurjchem-1477	193	6	1.5	1.5	NUM
eurjchem-1477	193	7	mmol	mmol	NOUN
eurjchem-1477	193	8	of	of	ADP
eurjchem-1477	193	9	reagent	reagent	NOUN
eurjchem-1477	193	10	was	be	AUX
eurjchem-1477	193	11	sufficient	sufficient	ADJ
eurjchem-1477	193	12	enough	enough	ADV
eurjchem-1477	193	13	for	for	ADP
eurjchem-1477	193	14	the	the	DET
eurjchem-1477	193	15	completion	completion	NOUN
eurjchem-1477	193	16	of	of	ADP
eurjchem-1477	193	17	reaction	reaction	NOUN
eurjchem-1477	193	18	with	with	ADP
eurjchem-1477	193	19	excellent	excellent	ADJ
eurjchem-1477	193	20	yield	yield	NOUN
eurjchem-1477	193	21	.	.	PUNCT
eurjchem-1477	194	1	further	far	ADV
eurjchem-1477	194	2	to	to	PART
eurjchem-1477	194	3	check	check	VERB
eurjchem-1477	194	4	the	the	DET
eurjchem-1477	194	5	effect	effect	NOUN
eurjchem-1477	194	6	of	of	ADP
eurjchem-1477	194	7	solvent	solvent	NOUN
eurjchem-1477	194	8	,	,	PUNCT
eurjchem-1477	194	9	we	we	PRON
eurjchem-1477	194	10	performed	perform	VERB
eurjchem-1477	194	11	cyclisation	cyclisation	NOUN
eurjchem-1477	194	12	reaction	reaction	NOUN
eurjchem-1477	194	13	with	with	ADP
eurjchem-1477	194	14	different	different	ADJ
eurjchem-1477	194	15	solvents	solvent	NOUN
eurjchem-1477	194	16	at	at	ADP
eurjchem-1477	194	17	room	room	NOUN
eurjchem-1477	194	18	tempera‐	tempera‐	PROPN
eurjchem-1477	194	19	ture	ture	PROPN
eurjchem-1477	194	20	.	.	PUNCT
eurjchem-1477	195	1	when	when	SCONJ
eurjchem-1477	195	2	the	the	DET
eurjchem-1477	195	3	reaction	reaction	NOUN
eurjchem-1477	195	4	was	be	AUX
eurjchem-1477	195	5	conducted	conduct	VERB
eurjchem-1477	195	6	using	use	VERB
eurjchem-1477	195	7	1.5	1.5	NUM
eurjchem-1477	195	8	mmol	mmol	NOUN
eurjchem-1477	195	9	of	of	ADP
eurjchem-1477	195	10	eaton	eaton	PROPN
eurjchem-1477	195	11	’s	’s	PART
eurjchem-1477	195	12	reagent	reagent	NOUN
eurjchem-1477	195	13	in	in	ADP
eurjchem-1477	195	14	dichloromethane	dichloromethane	NOUN
eurjchem-1477	195	15	as	as	SCONJ
eurjchem-1477	195	16	solvent	solvent	NOUN
eurjchem-1477	195	17	required	require	VERB
eurjchem-1477	195	18	50	50	NUM
eurjchem-1477	195	19	min	min	NOUN
eurjchem-1477	195	20	for	for	ADP
eurjchem-1477	195	21	completion	completion	NOUN
eurjchem-1477	195	22	and	and	CCONJ
eurjchem-1477	195	23	the	the	DET
eurjchem-1477	195	24	product	product	NOUN
eurjchem-1477	195	25	3a	3a	NUM
eurjchem-1477	195	26	obtained	obtain	VERB
eurjchem-1477	195	27	in	in	ADP
eurjchem-1477	195	28	70	70	NUM
eurjchem-1477	195	29	%	%	NOUN
eurjchem-1477	195	30	yield	yield	NOUN
eurjchem-1477	195	31	(	(	PUNCT
eurjchem-1477	195	32	table	table	NOUN
eurjchem-1477	195	33	3	3	NUM
eurjchem-1477	195	34	,	,	PUNCT
eurjchem-1477	195	35	entry	entry	NOUN
eurjchem-1477	195	36	1	1	NUM
eurjchem-1477	195	37	)	)	PUNCT
eurjchem-1477	195	38	.	.	PUNCT
eurjchem-1477	196	1	further	far	ADV
eurjchem-1477	196	2	42	42	NUM
eurjchem-1477	196	3	min	min	NOUN
eurjchem-1477	196	4	and	and	CCONJ
eurjchem-1477	196	5	60	60	NUM
eurjchem-1477	196	6	min	min	NOUN
eurjchem-1477	196	7	required	require	VERB
eurjchem-1477	196	8	for	for	ADP
eurjchem-1477	196	9	the	the	DET
eurjchem-1477	196	10	completion	completion	NOUN
eurjchem-1477	196	11	of	of	ADP
eurjchem-1477	196	12	reaction	reaction	NOUN
eurjchem-1477	196	13	when	when	SCONJ
eurjchem-1477	196	14	dichloroethane	dichloroethane	PROPN
eurjchem-1477	196	15	and	and	CCONJ
eurjchem-1477	196	16	tetrahydro‐	tetrahydro‐	PRON
eurjchem-1477	196	17	furan	furan	PROPN
eurjchem-1477	196	18	solvent	solvent	NOUN
eurjchem-1477	196	19	were	be	AUX
eurjchem-1477	196	20	used	use	VERB
eurjchem-1477	196	21	with	with	ADP
eurjchem-1477	196	22	63	63	NUM
eurjchem-1477	196	23	and	and	CCONJ
eurjchem-1477	196	24	78	78	NUM
eurjchem-1477	196	25	%	%	NOUN
eurjchem-1477	196	26	yield	yield	NOUN
eurjchem-1477	196	27	,	,	PUNCT
eurjchem-1477	196	28	respectively	respectively	ADV
eurjchem-1477	196	29	(	(	PUNCT
eurjchem-1477	196	30	table	table	NOUN
eurjchem-1477	196	31	3	3	NUM
eurjchem-1477	196	32	,	,	PUNCT
eurjchem-1477	196	33	entry	entry	NOUN
eurjchem-1477	196	34	2	2	NUM
eurjchem-1477	196	35	and	and	CCONJ
eurjchem-1477	196	36	3	3	NUM
eurjchem-1477	196	37	)	)	PUNCT
eurjchem-1477	196	38	.	.	PUNCT
eurjchem-1477	197	1	while	while	SCONJ
eurjchem-1477	197	2	on	on	ADP
eurjchem-1477	197	3	the	the	DET
eurjchem-1477	197	4	other	other	ADJ
eurjchem-1477	197	5	hand	hand	NOUN
eurjchem-1477	197	6	,	,	PUNCT
eurjchem-1477	197	7	when	when	SCONJ
eurjchem-1477	197	8	the	the	DET
eurjchem-1477	197	9	reaction	reaction	NOUN
eurjchem-1477	197	10	was	be	AUX
eurjchem-1477	197	11	carried	carry	VERB
eurjchem-1477	197	12	out	out	ADP
eurjchem-1477	197	13	using	use	VERB
eurjchem-1477	197	14	toluene	toluene	ADJ
eurjchem-1477	197	15	solvent	solvent	NOUN
eurjchem-1477	197	16	it	it	PRON
eurjchem-1477	197	17	takes	take	VERB
eurjchem-1477	197	18	70	70	NUM
eurjchem-1477	197	19	min	min	NOUN
eurjchem-1477	197	20	for	for	ADP
eurjchem-1477	197	21	the	the	DET
eurjchem-1477	197	22	completion	completion	NOUN
eurjchem-1477	197	23	with	with	ADP
eurjchem-1477	197	24	58	58	NUM
eurjchem-1477	197	25	%	%	NOUN
eurjchem-1477	197	26	yield	yield	NOUN
eurjchem-1477	197	27	(	(	PUNCT
eurjchem-1477	197	28	table	table	NOUN
eurjchem-1477	197	29	3	3	NUM
eurjchem-1477	197	30	,	,	PUNCT
eurjchem-1477	197	31	entry	entry	NOUN
eurjchem-1477	197	32	4	4	NUM
eurjchem-1477	197	33	)	)	PUNCT
eurjchem-1477	197	34	.	.	PUNCT
eurjchem-1477	198	1	finally	finally	ADV
eurjchem-1477	198	2	,	,	PUNCT
eurjchem-1477	198	3	when	when	SCONJ
eurjchem-1477	198	4	the	the	DET
eurjchem-1477	198	5	reaction	reaction	NOUN
eurjchem-1477	198	6	was	be	AUX
eurjchem-1477	198	7	performed	perform	VERB
eurjchem-1477	198	8	without	without	ADP
eurjchem-1477	198	9	any	any	DET
eurjchem-1477	198	10	solvent	solvent	NOUN
eurjchem-1477	198	11	it	it	PRON
eurjchem-1477	198	12	was	be	AUX
eurjchem-1477	198	13	completed	complete	VERB
eurjchem-1477	198	14	within	within	ADP
eurjchem-1477	198	15	10‐15	10‐15	NUM
eurjchem-1477	198	16	min	min	NOUN
eurjchem-1477	198	17	and	and	CCONJ
eurjchem-1477	198	18	product	product	NOUN
eurjchem-1477	198	19	obtained	obtain	VERB
eurjchem-1477	198	20	in	in	ADP
eurjchem-1477	198	21	93	93	NUM
eurjchem-1477	198	22	%	%	NOUN
eurjchem-1477	198	23	yield	yield	NOUN
eurjchem-1477	198	24	(	(	PUNCT
eurjchem-1477	198	25	table	table	NOUN
eurjchem-1477	198	26	3	3	NUM
eurjchem-1477	198	27	,	,	PUNCT
eurjchem-1477	198	28	entry	entry	NOUN
eurjchem-1477	198	29	5	5	NUM
eurjchem-1477	198	30	)	)	PUNCT
eurjchem-1477	198	31	.	.	PUNCT
eurjchem-1477	199	1	however	however	ADV
eurjchem-1477	199	2	to	to	PART
eurjchem-1477	199	3	check	check	VERB
eurjchem-1477	199	4	the	the	DET
eurjchem-1477	199	5	effect	effect	NOUN
eurjchem-1477	199	6	of	of	ADP
eurjchem-1477	199	7	temperature	temperature	NOUN
eurjchem-1477	199	8	on	on	ADP
eurjchem-1477	199	9	the	the	DET
eurjchem-1477	199	10	reaction	reaction	NOUN
eurjchem-1477	199	11	condition	condition	NOUN
eurjchem-1477	199	12	,	,	PUNCT
eurjchem-1477	199	13	reaction	reaction	NOUN
eurjchem-1477	199	14	was	be	AUX
eurjchem-1477	199	15	heated	heat	VERB
eurjchem-1477	199	16	with	with	ADP
eurjchem-1477	199	17	or	or	CCONJ
eurjchem-1477	199	18	without	without	ADP
eurjchem-1477	199	19	solvent	solvent	ADJ
eurjchem-1477	199	20	many	many	ADJ
eurjchem-1477	199	21	spots	spot	NOUN
eurjchem-1477	199	22	were	be	AUX
eurjchem-1477	199	23	observed	observe	VERB
eurjchem-1477	199	24	on	on	ADP
eurjchem-1477	199	25	tlc	tlc	NOUN
eurjchem-1477	199	26	along	along	ADP
eurjchem-1477	199	27	with	with	ADP
eurjchem-1477	199	28	product	product	NOUN
eurjchem-1477	199	29	spot	spot	NOUN
eurjchem-1477	199	30	and	and	CCONJ
eurjchem-1477	199	31	hence	hence	ADV
eurjchem-1477	199	32	yield	yield	NOUN
eurjchem-1477	199	33	of	of	ADP
eurjchem-1477	199	34	compound	compound	NOUN
eurjchem-1477	199	35	3a	3a	NUM
eurjchem-1477	199	36	was	be	AUX
eurjchem-1477	199	37	very	very	ADV
eurjchem-1477	199	38	poor	poor	ADJ
eurjchem-1477	199	39	.	.	PUNCT
eurjchem-1477	200	1	however	however	ADV
eurjchem-1477	200	2	to	to	PART
eurjchem-1477	200	3	explore	explore	VERB
eurjchem-1477	200	4	the	the	DET
eurjchem-1477	200	5	scope	scope	NOUN
eurjchem-1477	200	6	and	and	CCONJ
eurjchem-1477	200	7	limitations	limitation	NOUN
eurjchem-1477	200	8	of	of	ADP
eurjchem-1477	200	9	developed	develop	VERB
eurjchem-1477	200	10	methodology	methodology	NOUN
eurjchem-1477	200	11	,	,	PUNCT
eurjchem-1477	200	12	we	we	PRON
eurjchem-1477	200	13	extended	extend	VERB
eurjchem-1477	200	14	the	the	DET
eurjchem-1477	200	15	procedure	procedure	NOUN
eurjchem-1477	200	16	to	to	ADP
eurjchem-1477	200	17	various	various	ADJ
eurjchem-1477	200	18	substi‐	substi‐	PROPN
eurjchem-1477	200	19	tuted	tut	VERB
eurjchem-1477	200	20	phenylacetamide	phenylacetamide	ADV
eurjchem-1477	200	21	analogues	analogue	NOUN
eurjchem-1477	200	22	possessing	possess	VERB
eurjchem-1477	200	23	either	either	CCONJ
eurjchem-1477	200	24	electron	electron	NOUN
eurjchem-1477	200	25	donating	donating	NOUN
eurjchem-1477	200	26	or	or	CCONJ
eurjchem-1477	200	27	electron	electron	NOUN
eurjchem-1477	200	28	withdrawing	withdraw	VERB
eurjchem-1477	200	29	groups	group	NOUN
eurjchem-1477	200	30	at	at	ADP
eurjchem-1477	200	31	different	different	ADJ
eurjchem-1477	200	32	positions	position	NOUN
eurjchem-1477	200	33	and	and	CCONJ
eurjchem-1477	200	34	obtained	obtain	VERB
eurjchem-1477	200	35	results	result	NOUN
eurjchem-1477	200	36	are	be	AUX
eurjchem-1477	200	37	tabulated	tabulate	VERB
eurjchem-1477	200	38	as	as	ADP
eurjchem-1477	200	39	in	in	ADP
eurjchem-1477	200	40	table	table	NOUN
eurjchem-1477	200	41	4	4	NUM
eurjchem-1477	200	42	.	.	PUNCT
eurjchem-1477	201	1	it	it	PRON
eurjchem-1477	201	2	is	be	AUX
eurjchem-1477	201	3	observed	observe	VERB
eurjchem-1477	201	4	that	that	SCONJ
eurjchem-1477	201	5	the	the	DET
eurjchem-1477	201	6	phenylacetamides	phenylacetamide	NOUN
eurjchem-1477	201	7	possessing	possess	VERB
eurjchem-1477	201	8	electron	electron	NOUN
eurjchem-1477	201	9	withdrawing	withdraw	VERB
eurjchem-1477	201	10	groups	group	NOUN
eurjchem-1477	201	11	on	on	ADP
eurjchem-1477	201	12	the	the	DET
eurjchem-1477	201	13	aromatic	aromatic	ADJ
eurjchem-1477	201	14	ring	ring	NOUN
eurjchem-1477	201	15	(	(	PUNCT
eurjchem-1477	201	16	table	table	NOUN
eurjchem-1477	201	17	4	4	NUM
eurjchem-1477	201	18	,	,	PUNCT
eurjchem-1477	201	19	entry	entry	NOUN
eurjchem-1477	201	20	3d	3d	NOUN
eurjchem-1477	201	21	,	,	PUNCT
eurjchem-1477	201	22	3e	3e	NUM
eurjchem-1477	201	23	,	,	PUNCT
eurjchem-1477	201	24	3f	3f	NUM
eurjchem-1477	201	25	,	,	PUNCT
eurjchem-1477	201	26	3	3	NUM
eurjchem-1477	201	27	g	g	NOUN
eurjchem-1477	201	28	,	,	PUNCT
eurjchem-1477	201	29	3h	3h	NUM
eurjchem-1477	201	30	,	,	PUNCT
eurjchem-1477	201	31	3i	3i	NOUN
eurjchem-1477	201	32	and	and	CCONJ
eurjchem-1477	201	33	3j	3j	NUM
eurjchem-1477	201	34	)	)	PUNCT
eurjchem-1477	201	35	react	react	VERB
eurjchem-1477	201	36	faster	fast	ADV
eurjchem-1477	201	37	than	than	ADP
eurjchem-1477	201	38	the	the	DET
eurjchem-1477	201	39	electron	electron	NOUN
eurjchem-1477	201	40	donating	donate	VERB
eurjchem-1477	201	41	groups	group	NOUN
eurjchem-1477	201	42	(	(	PUNCT
eurjchem-1477	201	43	table	table	NOUN
eurjchem-1477	201	44	4	4	NUM
eurjchem-1477	201	45	,	,	PUNCT
eurjchem-1477	201	46	entry	entry	NOUN
eurjchem-1477	201	47	3a	3a	NUM
eurjchem-1477	201	48	,	,	PUNCT
eurjchem-1477	201	49	3b	3b	NUM
eurjchem-1477	201	50	,	,	PUNCT
eurjchem-1477	201	51	3c	3c	NUM
eurjchem-1477	201	52	and	and	CCONJ
eurjchem-1477	201	53	3k	3k	NUM
eurjchem-1477	201	54	)	)	PUNCT
eurjchem-1477	201	55	and	and	CCONJ
eurjchem-1477	201	56	we	we	PRON
eurjchem-1477	201	57	found	find	VERB
eurjchem-1477	201	58	that	that	SCONJ
eurjchem-1477	201	59	the	the	DET
eurjchem-1477	201	60	reaction	reaction	NOUN
eurjchem-1477	201	61	proceeds	proceed	VERB
eurjchem-1477	201	62	very	very	ADV
eurjchem-1477	201	63	efficiently	efficiently	ADV
eurjchem-1477	201	64	with	with	ADP
eurjchem-1477	201	65	all	all	DET
eurjchem-1477	201	66	the	the	DET
eurjchem-1477	201	67	cases	case	NOUN
eurjchem-1477	201	68	and	and	CCONJ
eurjchem-1477	201	69	products	product	NOUN
eurjchem-1477	201	70	obtained	obtain	VERB
eurjchem-1477	201	71	in	in	ADP
eurjchem-1477	201	72	high	high	ADJ
eurjchem-1477	201	73	yield	yield	NOUN
eurjchem-1477	201	74	.	.	PUNCT
eurjchem-1477	202	1	thimmaiah	thimmaiah	PROPN
eurjchem-1477	202	2	et	et	PROPN
eurjchem-1477	202	3	al	al	PROPN
eurjchem-1477	202	4	.	.	PUNCT
eurjchem-1477	202	5	/	/	SYM
eurjchem-1477	202	6	european	european	PROPN
eurjchem-1477	202	7	journal	journal	PROPN
eurjchem-1477	202	8	of	of	ADP
eurjchem-1477	202	9	chemistry	chemistry	NOUN
eurjchem-1477	202	10	7	7	NUM
eurjchem-1477	202	11	(	(	PUNCT
eurjchem-1477	202	12	4	4	NUM
eurjchem-1477	202	13	)	)	PUNCT
eurjchem-1477	202	14	(	(	PUNCT
eurjchem-1477	202	15	2016	2016	NUM
eurjchem-1477	202	16	)	)	PUNCT
eurjchem-1477	202	17	391‐396	391‐396	NUM
eurjchem-1477	202	18	395	395	NUM
eurjchem-1477	202	19	table	table	NOUN
eurjchem-1477	202	20	3	3	NUM
eurjchem-1477	202	21	.	.	PUNCT
eurjchem-1477	202	22	effect	effect	NOUN
eurjchem-1477	202	23	of	of	ADP
eurjchem-1477	202	24	solvent	solvent	NOUN
eurjchem-1477	202	25	on	on	ADP
eurjchem-1477	202	26	the	the	DET
eurjchem-1477	202	27	synthesis	synthesis	NOUN
eurjchem-1477	202	28	of	of	ADP
eurjchem-1477	202	29	8‐methoxy‐1,3‐dihydro‐benzo[d]azepin‐2‐one	8‐methoxy‐1,3‐dihydro‐benzo[d]azepin‐2‐one	NUM
eurjchem-1477	202	30	(	(	PUNCT
eurjchem-1477	202	31	3a	3a	NUM
eurjchem-1477	202	32	)	)	PUNCT
eurjchem-1477	202	33	*	*	PUNCT
eurjchem-1477	202	34	.	.	PUNCT
eurjchem-1477	203	1	entry	entry	NOUN
eurjchem-1477	203	2	solvent	solvent	ADJ
eurjchem-1477	203	3	time	time	NOUN
eurjchem-1477	203	4	(	(	PUNCT
eurjchem-1477	203	5	min	min	NOUN
eurjchem-1477	203	6	)	)	PUNCT
eurjchem-1477	203	7	yield	yield	NOUN
eurjchem-1477	203	8	(	(	PUNCT
eurjchem-1477	203	9	%	%	NOUN
eurjchem-1477	203	10	)	)	PUNCT
eurjchem-1477	203	11	1	1	NUM
eurjchem-1477	203	12	dichloromethane	dichloromethane	NOUN
eurjchem-1477	203	13	50	50	NUM
eurjchem-1477	203	14	70	70	NUM
eurjchem-1477	203	15	2	2	NUM
eurjchem-1477	203	16	dichloroethane	dichloroethane	NOUN
eurjchem-1477	203	17	60	60	NUM
eurjchem-1477	203	18	63	63	NUM
eurjchem-1477	203	19	3	3	NUM
eurjchem-1477	203	20	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-1477	203	21	42	42	NUM
eurjchem-1477	203	22	78	78	NUM
eurjchem-1477	203	23	4	4	NUM
eurjchem-1477	203	24	toluene	toluene	NOUN
eurjchem-1477	203	25	70	70	NUM
eurjchem-1477	203	26	58	58	NUM
eurjchem-1477	203	27	5	5	NUM
eurjchem-1477	203	28	solvent	solvent	NOUN
eurjchem-1477	203	29	free	free	ADJ
eurjchem-1477	203	30	10‐15	10‐15	NUM
eurjchem-1477	204	1	93	93	NUM
eurjchem-1477	204	2	*	*	SYM
eurjchem-1477	204	3	1.5	1.5	NUM
eurjchem-1477	204	4	mmol	mmol	NOUN
eurjchem-1477	204	5	of	of	ADP
eurjchem-1477	204	6	eaton	eaton	PROPN
eurjchem-1477	204	7	’s	’s	PART
eurjchem-1477	204	8	reagent	reagent	NOUN
eurjchem-1477	204	9	used	use	VERB
eurjchem-1477	204	10	along	along	ADP
eurjchem-1477	204	11	with	with	ADP
eurjchem-1477	204	12	solvent	solvent	NOUN
eurjchem-1477	204	13	;	;	PUNCT
eurjchem-1477	204	14	reaction	reaction	NOUN
eurjchem-1477	204	15	condition	condition	NOUN
eurjchem-1477	204	16	:	:	PUNCT
eurjchem-1477	204	17	room	room	NOUN
eurjchem-1477	204	18	temperature	temperature	NOUN
eurjchem-1477	204	19	,	,	PUNCT
eurjchem-1477	204	20	0.39	0.39	NUM
eurjchem-1477	204	21	mmol	mmol	NOUN
eurjchem-1477	204	22	of	of	ADP
eurjchem-1477	204	23	compound	compound	NOUN
eurjchem-1477	204	24	2a	2a	NUM
eurjchem-1477	204	25	.	.	PUNCT
eurjchem-1477	205	1	table	table	NOUN
eurjchem-1477	205	2	4	4	NUM
eurjchem-1477	205	3	.	.	PUNCT
eurjchem-1477	205	4	structures	structure	NOUN
eurjchem-1477	205	5	of	of	ADP
eurjchem-1477	205	6	synthesized	synthesize	VERB
eurjchem-1477	205	7	3‐benzazepinones	3‐benzazepinones	NUM
eurjchem-1477	205	8	3a‐k	3a‐k	NOUN
eurjchem-1477	205	9	.	.	PUNCT
eurjchem-1477	206	1	compound	compound	NOUN
eurjchem-1477	206	2	structure	structure	NOUN
eurjchem-1477	206	3	time	time	NOUN
eurjchem-1477	206	4	(	(	PUNCT
eurjchem-1477	206	5	min	min	NOUN
eurjchem-1477	206	6	)	)	PUNCT
eurjchem-1477	206	7	yield	yield	NOUN
eurjchem-1477	206	8	(	(	PUNCT
eurjchem-1477	206	9	%	%	INTJ
eurjchem-1477	206	10	)	)	PUNCT
eurjchem-1477	206	11	*	*	PUNCT
eurjchem-1477	207	1	3a	3a	NUM
eurjchem-1477	207	2	13‐14	13‐14	NUM
eurjchem-1477	207	3	90	90	NUM
eurjchem-1477	207	4	3b	3b	NUM
eurjchem-1477	207	5	14	14	NUM
eurjchem-1477	207	6	89	89	NUM
eurjchem-1477	207	7	3c	3c	NUM
eurjchem-1477	207	8	14	14	NUM
eurjchem-1477	207	9	85	85	NUM
eurjchem-1477	207	10	3d	3d	NOUN
eurjchem-1477	208	1	9‐10	9‐10	NUM
eurjchem-1477	208	2	93	93	NUM
eurjchem-1477	208	3	3e	3e	NOUN
eurjchem-1477	208	4	nh	nh	PROPN
eurjchem-1477	209	1	f	f	PROPN
eurjchem-1477	209	2	o	o	NOUN
eurjchem-1477	209	3	9	9	NUM
eurjchem-1477	209	4	92	92	NUM
eurjchem-1477	209	5	3f	3f	PROPN
eurjchem-1477	209	6	13	13	NUM
eurjchem-1477	209	7	90	90	NUM
eurjchem-1477	209	8	3	3	NUM
eurjchem-1477	209	9	g	g	NOUN
eurjchem-1477	209	10	12	12	NUM
eurjchem-1477	209	11	92	92	NUM
eurjchem-1477	209	12	3h	3h	NUM
eurjchem-1477	209	13	12	12	NUM
eurjchem-1477	209	14	93	93	NUM
eurjchem-1477	209	15	3i	3i	NUM
eurjchem-1477	209	16	13	13	NUM
eurjchem-1477	209	17	91	91	NUM
eurjchem-1477	209	18	3j	3j	NOUN
eurjchem-1477	209	19	9	9	NUM
eurjchem-1477	209	20	90	90	NUM
eurjchem-1477	209	21	3k	3k	NUM
eurjchem-1477	209	22	nh	nh	NOUN
eurjchem-1477	210	1	o	o	NOUN
eurjchem-1477	210	2	o	o	X
eurjchem-1477	210	3	o	o	NOUN
eurjchem-1477	210	4	15	15	NUM
eurjchem-1477	210	5	85	85	NUM
eurjchem-1477	210	6	*	*	NUM
eurjchem-1477	210	7	isolated	isolated	ADJ
eurjchem-1477	210	8	yield	yield	NOUN
eurjchem-1477	210	9	;	;	PUNCT
eurjchem-1477	210	10	reaction	reaction	NOUN
eurjchem-1477	210	11	condition	condition	NOUN
eurjchem-1477	210	12	:	:	PUNCT
eurjchem-1477	210	13	room	room	NOUN
eurjchem-1477	210	14	temperature	temperature	NOUN
eurjchem-1477	210	15	,	,	PUNCT
eurjchem-1477	210	16	solvent	solvent	NOUN
eurjchem-1477	210	17	free	free	ADJ
eurjchem-1477	210	18	,	,	PUNCT
eurjchem-1477	210	19	1.5	1.5	NUM
eurjchem-1477	210	20	mmol	mmol	NOUN
eurjchem-1477	210	21	of	of	ADP
eurjchem-1477	210	22	eaton	eaton	PROPN
eurjchem-1477	210	23	’s	’s	PART
eurjchem-1477	210	24	reagent	reagent	NOUN
eurjchem-1477	210	25	.	.	PUNCT
eurjchem-1477	211	1	4	4	X
eurjchem-1477	211	2	.	.	X
eurjchem-1477	211	3	conclusion	conclusion	NOUN
eurjchem-1477	211	4	in	in	ADP
eurjchem-1477	211	5	conclusion	conclusion	NOUN
eurjchem-1477	211	6	,	,	PUNCT
eurjchem-1477	211	7	for	for	ADP
eurjchem-1477	211	8	the	the	DET
eurjchem-1477	211	9	first	first	ADJ
eurjchem-1477	211	10	time	time	NOUN
eurjchem-1477	211	11	we	we	PRON
eurjchem-1477	211	12	have	have	AUX
eurjchem-1477	211	13	demonstrated	demonstrate	VERB
eurjchem-1477	211	14	an	an	DET
eurjchem-1477	211	15	excellent	excellent	ADJ
eurjchem-1477	211	16	,	,	PUNCT
eurjchem-1477	211	17	mild	mild	ADJ
eurjchem-1477	211	18	and	and	CCONJ
eurjchem-1477	211	19	efficient	efficient	ADJ
eurjchem-1477	211	20	protocol	protocol	NOUN
eurjchem-1477	211	21	for	for	ADP
eurjchem-1477	211	22	the	the	DET
eurjchem-1477	211	23	synthesis	synthesis	NOUN
eurjchem-1477	211	24	of	of	ADP
eurjchem-1477	211	25	3‐	3‐	NUM
eurjchem-1477	211	26	benzazepinones	benzazepinone	NOUN
eurjchem-1477	211	27	using	use	VERB
eurjchem-1477	211	28	eaton	eaton	PROPN
eurjchem-1477	211	29	’s	’s	PART
eurjchem-1477	211	30	reagent	reagent	NOUN
eurjchem-1477	211	31	.	.	PUNCT
eurjchem-1477	212	1	the	the	DET
eurjchem-1477	212	2	noteworthy	noteworthy	ADJ
eurjchem-1477	212	3	features	feature	NOUN
eurjchem-1477	212	4	of	of	ADP
eurjchem-1477	212	5	this	this	DET
eurjchem-1477	212	6	protocol	protocol	NOUN
eurjchem-1477	212	7	are	be	AUX
eurjchem-1477	212	8	shorter	short	ADJ
eurjchem-1477	212	9	reaction	reaction	NOUN
eurjchem-1477	212	10	time	time	NOUN
eurjchem-1477	212	11	,	,	PUNCT
eurjchem-1477	212	12	broad	broad	ADJ
eurjchem-1477	212	13	functional	functional	ADJ
eurjchem-1477	212	14	group	group	NOUN
eurjchem-1477	212	15	tolerance	tolerance	NOUN
eurjchem-1477	212	16	,	,	PUNCT
eurjchem-1477	212	17	and	and	CCONJ
eurjchem-1477	212	18	mild	mild	ADJ
eurjchem-1477	212	19	reaction	reaction	NOUN
eurjchem-1477	212	20	condition	condition	NOUN
eurjchem-1477	212	21	,	,	PUNCT
eurjchem-1477	212	22	avoiding	avoid	VERB
eurjchem-1477	212	23	hazardous	hazardous	ADJ
eurjchem-1477	212	24	organic	organic	ADJ
eurjchem-1477	212	25	solvent	solvent	NOUN
eurjchem-1477	212	26	and	and	CCONJ
eurjchem-1477	212	27	metal	metal	NOUN
eurjchem-1477	212	28	catalyst	catalyst	NOUN
eurjchem-1477	212	29	,	,	PUNCT
eurjchem-1477	212	30	green	green	ADJ
eurjchem-1477	212	31	aspects	aspect	NOUN
eurjchem-1477	212	32	,	,	PUNCT
eurjchem-1477	212	33	ease	ease	NOUN
eurjchem-1477	212	34	of	of	ADP
eurjchem-1477	212	35	product	product	NOUN
eurjchem-1477	212	36	purification	purification	NOUN
eurjchem-1477	212	37	along	along	ADP
eurjchem-1477	212	38	with	with	ADP
eurjchem-1477	212	39	excellent	excellent	ADJ
eurjchem-1477	212	40	yields	yield	NOUN
eurjchem-1477	212	41	.	.	PUNCT
eurjchem-1477	213	1	acknowledgements	acknowledgement	NOUN
eurjchem-1477	213	2	this	this	DET
eurjchem-1477	213	3	work	work	NOUN
eurjchem-1477	213	4	was	be	AUX
eurjchem-1477	213	5	supported	support	VERB
eurjchem-1477	213	6	to	to	ADP
eurjchem-1477	213	7	babu	babu	PROPN
eurjchem-1477	213	8	shubha	shubha	PROPN
eurjchem-1477	213	9	priya	priya	PROPN
eurjchem-1477	213	10	through	through	ADP
eurjchem-1477	213	11	financial	financial	ADJ
eurjchem-1477	213	12	assistance	assistance	NOUN
eurjchem-1477	213	13	from	from	ADP
eurjchem-1477	213	14	science	science	NOUN
eurjchem-1477	213	15	and	and	CCONJ
eurjchem-1477	213	16	engineering	engineering	NOUN
eurjchem-1477	213	17	research	research	NOUN
eurjchem-1477	213	18	board	board	NOUN
eurjchem-1477	213	19	,	,	PUNCT
eurjchem-1477	213	20	new	new	ADJ
eurjchem-1477	213	21	delhi	delhi	PROPN
eurjchem-1477	213	22	[	[	X
eurjchem-1477	213	23	start‐up‐research	start‐up‐research	NOUN
eurjchem-1477	213	24	grant	grant	NOUN
eurjchem-1477	213	25	(	(	PUNCT
eurjchem-1477	213	26	young	young	ADJ
eurjchem-1477	213	27	scientists)‐	scientists)‐	NOUN
eurjchem-1477	213	28	life	life	NOUN
eurjchem-1477	213	29	sciences	science	NOUN
eurjchem-1477	213	30	]	]	PUNCT
eurjchem-1477	214	1	no	no	NOUN
eurjchem-1477	214	2	:	:	PUNCT
eurjchem-1477	214	3	sb	sb	NOUN
eurjchem-1477	214	4	/	/	SYM
eurjchem-1477	214	5	ft	ft	PROPN
eurjchem-1477	214	6	/	/	SYM
eurjchem-1477	214	7	ls‐297/2012	ls‐297/2012	NOUN
eurjchem-1477	214	8	]	]	PUNCT
eurjchem-1477	214	9	and	and	CCONJ
eurjchem-1477	214	10	university	university	NOUN
eurjchem-1477	214	11	grants	grant	NOUN
eurjchem-1477	214	12	commission	commission	PROPN
eurjchem-1477	214	13	,	,	PUNCT
eurjchem-1477	214	14	new	new	ADJ
eurjchem-1477	214	15	delhi	delhi	PROPN
eurjchem-1477	214	16	,	,	PUNCT
eurjchem-1477	214	17	govt	govt	PROPN
eurjchem-1477	214	18	.	.	PUNCT
eurjchem-1477	215	1	of	of	ADP
eurjchem-1477	215	2	india	india	PROPN
eurjchem-1477	216	1	under	under	ADP
eurjchem-1477	216	2	ugc‐mrp	ugc‐mrp	PROPN
eurjchem-1477	216	3	vide	vide	NOUN
eurjchem-1477	216	4	no	no	PROPN
eurjchem-1477	216	5	.	.	PUNCT
eurjchem-1477	217	1	f.	f.	PROPN
eurjchem-1477	217	2	no	no	PRON
eurjchem-1477	217	3	:	:	PUNCT
eurjchem-1477	217	4	41/224/2012	41/224/2012	NUM
eurjchem-1477	217	5	(	(	PUNCT
eurjchem-1477	217	6	sr	sr	PROPN
eurjchem-1477	217	7	)	)	PUNCT
eurjchem-1477	217	8	.	.	PUNCT
eurjchem-1477	218	1	authors	author	NOUN
eurjchem-1477	218	2	thanks	thank	NOUN
eurjchem-1477	218	3	management	management	NOUN
eurjchem-1477	218	4	,	,	PUNCT
eurjchem-1477	218	5	cjex	cjex	NOUN
eurjchem-1477	218	6	biochem	biochem	PROPN
eurjchem-1477	218	7	pvt	pvt	PROPN
eurjchem-1477	218	8	.	.	PROPN
eurjchem-1477	218	9	ltd	ltd	PROPN
eurjchem-1477	218	10	.	.	PROPN
eurjchem-1477	218	11	bangalore	bangalore	PROPN
eurjchem-1477	218	12	for	for	ADP
eurjchem-1477	218	13	their	their	PRON
eurjchem-1477	218	14	continuous	continuous	ADJ
eurjchem-1477	218	15	support	support	NOUN
eurjchem-1477	218	16	for	for	ADP
eurjchem-1477	218	17	this	this	DET
eurjchem-1477	218	18	research	research	NOUN
eurjchem-1477	218	19	work	work	NOUN
eurjchem-1477	218	20	.	.	PUNCT
eurjchem-1477	219	1	ms	ms	PROPN
eurjchem-1477	219	2	.	.	PROPN
eurjchem-1477	219	3	shubhavathi	shubhavathi	PROPN
eurjchem-1477	219	4	thimmaiah	thimmaiah	PROPN
eurjchem-1477	219	5	is	be	AUX
eurjchem-1477	219	6	thankful	thankful	ADJ
eurjchem-1477	219	7	to	to	ADP
eurjchem-1477	219	8	university	university	NOUN
eurjchem-1477	219	9	of	of	ADP
eurjchem-1477	219	10	mysore	mysore	NOUN
eurjchem-1477	219	11	,	,	PUNCT
eurjchem-1477	219	12	mysuru	mysuru	PROPN
eurjchem-1477	219	13	,	,	PUNCT
eurjchem-1477	219	14	india	india	PROPN
eurjchem-1477	219	15	,	,	PUNCT
eurjchem-1477	219	16	for	for	ADP
eurjchem-1477	219	17	providing	provide	VERB
eurjchem-1477	219	18	financial	financial	ADJ
eurjchem-1477	219	19	support	support	NOUN
eurjchem-1477	219	20	under	under	ADP
eurjchem-1477	219	21	ugc‐non	ugc‐non	NUM
eurjchem-1477	219	22	net	net	ADJ
eurjchem-1477	219	23	fellowship	fellowship	NOUN
eurjchem-1477	219	24	scheme	scheme	NOUN
eurjchem-1477	219	25	,	,	PUNCT
eurjchem-1477	219	26	no	no	INTJ
eurjchem-1477	219	27	.	.	PUNCT
eurjchem-1477	220	1	dv9/192	dv9/192	PROPN
eurjchem-1477	220	2	/	/	SYM
eurjchem-1477	220	3	non‐netfs/2013‐14	non‐netfs/2013‐14	PROPN
eurjchem-1477	220	4	.	.	PUNCT
eurjchem-1477	221	1	references	reference	NOUN
eurjchem-1477	221	2	[	[	X
eurjchem-1477	221	3	1	1	NUM
eurjchem-1477	221	4	]	]	PUNCT
eurjchem-1477	221	5	.	.	PUNCT
eurjchem-1477	222	1	lewis	lewis	PROPN
eurjchem-1477	222	2	,	,	PUNCT
eurjchem-1477	222	3	h.	h.	PROPN
eurjchem-1477	222	4	d.	d.	PROPN
eurjchem-1477	222	5	;	;	PUNCT
eurjchem-1477	222	6	perez‐revuetta	perez‐revuetta	PROPN
eurjchem-1477	222	7	,	,	PUNCT
eurjchem-1477	222	8	b.	b.	PROPN
eurjchem-1477	222	9	i.	i.	PROPN
eurjchem-1477	222	10	;	;	PUNCT
eurjchem-1477	222	11	nadin	nadin	NOUN
eurjchem-1477	222	12	,	,	PUNCT
eurjchem-1477	222	13	a.	a.	NOUN
eurjchem-1477	222	14	;	;	PUNCT
eurjchem-1477	222	15	neduvelil	neduvelil	PROPN
eurjchem-1477	222	16	,	,	PUNCT
eurjchem-1477	222	17	j.	j.	PROPN
eurjchem-1477	222	18	g.	g.	PROPN
eurjchem-1477	222	19	;	;	PUNCT
eurjchem-1477	222	20	harrison	harrison	PROPN
eurjchem-1477	222	21	,	,	PUNCT
eurjchem-1477	222	22	t.	t.	PROPN
eurjchem-1477	222	23	;	;	PUNCT
eurjchem-1477	222	24	pollack	pollack	PROPN
eurjchem-1477	222	25	,	,	PUNCT
eurjchem-1477	222	26	s.	s.	PROPN
eurjchem-1477	222	27	j.	j.	PROPN
eurjchem-1477	222	28	;	;	PUNCT
eurjchem-1477	222	29	slearman	slearman	NOUN
eurjchem-1477	222	30	,	,	PUNCT
eurjchem-1477	222	31	m.	m.	NOUN
eurjchem-1477	222	32	s.	s.	PROPN
eurjchem-1477	222	33	biochemistry‐us	biochemistry‐us	PROPN
eurjchem-1477	222	34	.	.	PUNCT
eurjchem-1477	223	1	2003	2003	NUM
eurjchem-1477	223	2	,	,	PUNCT
eurjchem-1477	223	3	42	42	NUM
eurjchem-1477	223	4	,	,	PUNCT
eurjchem-1477	223	5	7580‐	7580‐	NUM
eurjchem-1477	223	6	7586	7586	NUM
eurjchem-1477	223	7	.	.	PUNCT
eurjchem-1477	224	1	[	[	X
eurjchem-1477	224	2	2	2	NUM
eurjchem-1477	224	3	]	]	PUNCT
eurjchem-1477	224	4	.	.	PUNCT
eurjchem-1477	225	1	bisi	bisi	PROPN
eurjchem-1477	225	2	,	,	PUNCT
eurjchem-1477	225	3	a.	a.	NOUN
eurjchem-1477	225	4	;	;	PUNCT
eurjchem-1477	225	5	rampa	rampa	PROPN
eurjchem-1477	225	6	,	,	PUNCT
eurjchem-1477	225	7	a.	a.	NOUN
eurjchem-1477	225	8	;	;	PUNCT
eurjchem-1477	225	9	badriesi	badriesi	PROPN
eurjchem-1477	225	10	,	,	PUNCT
eurjchem-1477	225	11	r.	r.	PROPN
eurjchem-1477	225	12	;	;	PUNCT
eurjchem-1477	225	13	gobbi	gobbi	PROPN
eurjchem-1477	225	14	,	,	PUNCT
eurjchem-1477	225	15	s.	s.	PROPN
eurjchem-1477	225	16	;	;	PUNCT
eurjchem-1477	225	17	belluti	belluti	NOUN
eurjchem-1477	225	18	,	,	PUNCT
eurjchem-1477	225	19	f.	f.	PROPN
eurjchem-1477	225	20	;	;	PUNCT
eurjchem-1477	225	21	loan	loan	NOUN
eurjchem-1477	225	22	,	,	PUNCT
eurjchem-1477	225	23	p.	p.	NOUN
eurjchem-1477	225	24	;	;	PUNCT
eurjchem-1477	225	25	varoti	varoti	PROPN
eurjchem-1477	225	26	,	,	PUNCT
eurjchem-1477	225	27	e.	e.	PROPN
eurjchem-1477	225	28	;	;	PUNCT
eurjchem-1477	225	29	chiarini	chiarini	PROPN
eurjchem-1477	225	30	,	,	PUNCT
eurjchem-1477	225	31	a.	a.	NOUN
eurjchem-1477	225	32	;	;	PUNCT
eurjchem-1477	225	33	valenti	valenti	PROPN
eurjchem-1477	225	34	,	,	PUNCT
eurjchem-1477	225	35	p.	p.	PROPN
eurjchem-1477	225	36	bioorg	bioorg	PROPN
eurjchem-1477	225	37	.	.	PUNCT
eurjchem-1477	226	1	med	med	PROPN
eurjchem-1477	226	2	.	.	PROPN
eurjchem-1477	226	3	chem	chem	PROPN
eurjchem-1477	226	4	.	.	PUNCT
eurjchem-1477	227	1	lett	lett	PROPN
eurjchem-1477	227	2	.	.	PUNCT
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eurjchem-1477	227	4	,	,	PUNCT
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eurjchem-1477	227	6	,	,	PUNCT
eurjchem-1477	227	7	1353‐	1353‐	NUM
eurjchem-1477	227	8	1361	1361	NUM
eurjchem-1477	227	9	.	.	PUNCT
eurjchem-1477	228	1	396	396	NUM
eurjchem-1477	228	2	thimmaiah	thimmaiah	PROPN
eurjchem-1477	228	3	et	et	PROPN
eurjchem-1477	228	4	al	al	PROPN
eurjchem-1477	228	5	.	.	PUNCT
eurjchem-1477	228	6	/	/	SYM
eurjchem-1477	228	7	european	european	PROPN
eurjchem-1477	228	8	journal	journal	PROPN
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eurjchem-1477	228	11	7	7	NUM
eurjchem-1477	228	12	(	(	PUNCT
eurjchem-1477	228	13	4	4	NUM
eurjchem-1477	228	14	)	)	PUNCT
eurjchem-1477	228	15	(	(	PUNCT
eurjchem-1477	228	16	2016	2016	NUM
eurjchem-1477	228	17	)	)	PUNCT
eurjchem-1477	228	18	391‐396	391‐396	NUM
eurjchem-1477	229	1	[	[	X
eurjchem-1477	229	2	3	3	NUM
eurjchem-1477	229	3	]	]	PUNCT
eurjchem-1477	229	4	.	.	PUNCT
eurjchem-1477	230	1	gnanalingaham	gnanalingaham	PROPN
eurjchem-1477	230	2	,	,	PUNCT
eurjchem-1477	230	3	k.	k.	PROPN
eurjchem-1477	230	4	k.	k.	PROPN
eurjchem-1477	230	5	;	;	PUNCT
eurjchem-1477	230	6	hunter	hunter	NOUN
eurjchem-1477	230	7	,	,	PUNCT
eurjchem-1477	230	8	a.	a.	PROPN
eurjchem-1477	230	9	j.	j.	PROPN
eurjchem-1477	230	10	;	;	PUNCT
eurjchem-1477	230	11	jenner	jenner	PROPN
eurjchem-1477	230	12	,	,	PUNCT
eurjchem-1477	230	13	p.	p.	PROPN
eurjchem-1477	230	14	;	;	PUNCT
eurjchem-1477	230	15	marsden	marsden	PROPN
eurjchem-1477	230	16	,	,	PUNCT
eurjchem-1477	230	17	c.	c.	PROPN
eurjchem-1477	230	18	d.	d.	PROPN
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eurjchem-1477	230	20	(	(	PUNCT
eurjchem-1477	230	21	berl	berl	PROPN
eurjchem-1477	230	22	)	)	PUNCT
eurjchem-1477	230	23	.	.	PUNCT
eurjchem-1477	231	1	1995	1995	NUM
eurjchem-1477	231	2	,	,	PUNCT
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eurjchem-1477	231	4	,	,	PUNCT
eurjchem-1477	231	5	403‐412	403‐412	PROPN
eurjchem-1477	231	6	.	.	PUNCT
eurjchem-1477	232	1	[	[	X
eurjchem-1477	232	2	4	4	NUM
eurjchem-1477	232	3	]	]	PUNCT
eurjchem-1477	232	4	.	.	PUNCT
eurjchem-1477	233	1	le‐diguarher	le‐diguarher	PROPN
eurjchem-1477	233	2	,	,	PUNCT
eurjchem-1477	233	3	t.	t.	PROPN
eurjchem-1477	233	4	;	;	PUNCT
eurjchem-1477	233	5	ortuno	ortuno	PROPN
eurjchem-1477	233	6	,	,	PUNCT
eurjchem-1477	233	7	j.	j.	PROPN
eurjchem-1477	233	8	c.	c.	PROPN
eurjchem-1477	233	9	;	;	PUNCT
eurjchem-1477	233	10	shanks	shank	NOUN
eurjchem-1477	233	11	,	,	PUNCT
eurjchem-1477	233	12	d.	d.	PROPN
eurjchem-1477	233	13	;	;	PUNCT
eurjchem-1477	233	14	guilbaud	guilbaud	PROPN
eurjchem-1477	233	15	,	,	PUNCT
eurjchem-1477	233	16	n.	n.	NOUN
eurjchem-1477	233	17	;	;	PUNCT
eurjchem-1477	233	18	pierre	pierre	PROPN
eurjchem-1477	233	19	,	,	PUNCT
eurjchem-1477	233	20	a.	a.	NOUN
eurjchem-1477	233	21	;	;	PUNCT
eurjchem-1477	233	22	raimbaud	raimbaud	VERB
eurjchem-1477	233	23	,	,	PUNCT
eurjchem-1477	233	24	e.	e.	PROPN
eurjchem-1477	233	25	;	;	PUNCT
eurjchem-1477	233	26	fauchere	fauchere	PROPN
eurjchem-1477	233	27	,	,	PUNCT
eurjchem-1477	233	28	j.	j.	PROPN
eurjchem-1477	233	29	l.	l.	PROPN
eurjchem-1477	233	30	;	;	PUNCT
eurjchem-1477	233	31	hickman	hickman	PROPN
eurjchem-1477	233	32	,	,	PUNCT
eurjchem-1477	233	33	j.	j.	PROPN
eurjchem-1477	233	34	a.	a.	PROPN
eurjchem-1477	233	35	;	;	PUNCT
eurjchem-1477	233	36	tucker	tucker	PROPN
eurjchem-1477	233	37	,	,	PUNCT
eurjchem-1477	233	38	g.	g.	PROPN
eurjchem-1477	233	39	c.	c.	PROPN
eurjchem-1477	233	40	;	;	PUNCT
eurjchem-1477	233	41	casara	casara	PROPN
eurjchem-1477	233	42	,	,	PUNCT
eurjchem-1477	233	43	p.	p.	PROPN
eurjchem-1477	233	44	j.	j.	PROPN
eurjchem-1477	233	45	bioorg	bioorg	PROPN
eurjchem-1477	233	46	.	.	PUNCT
eurjchem-1477	234	1	med	med	PROPN
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eurjchem-1477	234	4	.	.	PUNCT
eurjchem-1477	235	1	lett	lett	PROPN
eurjchem-1477	235	2	.	.	PUNCT
eurjchem-1477	236	1	2004	2004	NUM
eurjchem-1477	236	2	,	,	PUNCT
eurjchem-1477	236	3	14	14	NUM
eurjchem-1477	236	4	,	,	PUNCT
eurjchem-1477	236	5	767‐771	767‐771	NUM
eurjchem-1477	236	6	.	.	PUNCT
eurjchem-1477	237	1	[	[	X
eurjchem-1477	237	2	5	5	NUM
eurjchem-1477	237	3	]	]	PUNCT
eurjchem-1477	237	4	.	.	PUNCT
eurjchem-1477	238	1	daemmgen	daemmgen	PROPN
eurjchem-1477	238	2	,	,	PUNCT
eurjchem-1477	238	3	j.	j.	PROPN
eurjchem-1477	238	4	;	;	PUNCT
eurjchem-1477	238	5	guth	guth	PROPN
eurjchem-1477	238	6	,	,	PUNCT
eurjchem-1477	238	7	b.	b.	PROPN
eurjchem-1477	238	8	;	;	PUNCT
eurjchem-1477	238	9	seidler	seidler	NOUN
eurjchem-1477	238	10	,	,	PUNCT
eurjchem-1477	238	11	r.	r.	PROPN
eurjchem-1477	238	12	wo	will	AUX
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eurjchem-1477	238	14	a2	a2	PROPN
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eurjchem-1477	238	16	:	:	PUNCT
eurjchem-1477	238	17	pct	pct	NOUN
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eurjchem-1477	238	19	.	.	PUNCT
eurjchem-1477	239	1	appl	appl	PROPN
eurjchem-1477	239	2	.	.	PROPN
eurjchem-1477	240	1	2001	2001	NUM
eurjchem-1477	240	2	,	,	PUNCT
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eurjchem-1477	240	4	.	.	PUNCT
eurjchem-1477	241	1	[	[	X
eurjchem-1477	241	2	6	6	NUM
eurjchem-1477	241	3	]	]	PUNCT
eurjchem-1477	241	4	.	.	PUNCT
eurjchem-1477	242	1	reiffen	reiffen	NOUN
eurjchem-1477	242	2	,	,	PUNCT
eurjchem-1477	242	3	m.	m.	NOUN
eurjchem-1477	242	4	;	;	PUNCT
eurjchem-1477	242	5	eberlein	eberlein	PROPN
eurjchem-1477	242	6	,	,	PUNCT
eurjchem-1477	242	7	w.	w.	PROPN
eurjchem-1477	242	8	;	;	PUNCT
eurjchem-1477	242	9	muller	muller	PROPN
eurjchem-1477	242	10	,	,	PUNCT
eurjchem-1477	242	11	p.	p.	PROPN
eurjchem-1477	242	12	;	;	PUNCT
eurjchem-1477	242	13	psiorz	psiorz	NOUN
eurjchem-1477	242	14	,	,	PUNCT
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eurjchem-1477	242	16	;	;	PUNCT
eurjchem-1477	242	17	noll	noll	PROPN
eurjchem-1477	242	18	,	,	PUNCT
eurjchem-1477	242	19	k.	k.	PROPN
eurjchem-1477	242	20	;	;	PUNCT
eurjchem-1477	242	21	heider	heider	NOUN
eurjchem-1477	242	22	,	,	PUNCT
eurjchem-1477	242	23	j.	j.	PROPN
eurjchem-1477	242	24	;	;	PUNCT
eurjchem-1477	242	25	lillie	lillie	PROPN
eurjchem-1477	242	26	,	,	PUNCT
eurjchem-1477	242	27	c.	c.	PROPN
eurjchem-1477	242	28	;	;	PUNCT
eurjchem-1477	242	29	kobinger	kobinger	PROPN
eurjchem-1477	242	30	,	,	PUNCT
eurjchem-1477	242	31	w.	w.	PROPN
eurjchem-1477	242	32	;	;	PUNCT
eurjchem-1477	242	33	luger	luger	PROPN
eurjchem-1477	242	34	,	,	PUNCT
eurjchem-1477	242	35	p.	p.	PROPN
eurjchem-1477	242	36	j.	j.	PROPN
eurjchem-1477	242	37	med	med	PROPN
eurjchem-1477	242	38	.	.	PROPN
eurjchem-1477	242	39	chem	chem	PROPN
eurjchem-1477	242	40	.	.	PUNCT
eurjchem-1477	243	1	1990	1990	NUM
eurjchem-1477	243	2	,	,	PUNCT
eurjchem-1477	243	3	33	33	NUM
eurjchem-1477	243	4	,	,	PUNCT
eurjchem-1477	243	5	1496‐1504	1496‐1504	NUM
eurjchem-1477	243	6	.	.	PUNCT
eurjchem-1477	244	1	[	[	X
eurjchem-1477	244	2	7	7	NUM
eurjchem-1477	244	3	]	]	PUNCT
eurjchem-1477	244	4	.	.	PUNCT
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eurjchem-1477	245	2	,	,	PUNCT
eurjchem-1477	245	3	p.	p.	NOUN
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eurjchem-1477	245	5	u.	u.	PROPN
eurjchem-1477	245	6	s.	s.	PROPN
eurjchem-1477	245	7	patent	patent	PROPN
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eurjchem-1477	245	9	,	,	PUNCT
eurjchem-1477	245	10	2008	2008	NUM
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eurjchem-1477	246	1	[	[	X
eurjchem-1477	246	2	8	8	NUM
eurjchem-1477	246	3	]	]	PUNCT
eurjchem-1477	246	4	.	.	PUNCT
eurjchem-1477	247	1	giles	giles	PROPN
eurjchem-1477	247	2	,	,	PUNCT
eurjchem-1477	247	3	b.	b.	PROPN
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eurjchem-1477	247	5	u.	u.	PROPN
eurjchem-1477	247	6	s.	s.	PROPN
eurjchem-1477	247	7	patent	patent	PROPN
eurjchem-1477	247	8	0038376	0038376	PROPN
eurjchem-1477	247	9	,	,	PUNCT
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eurjchem-1477	248	1	[	[	X
eurjchem-1477	248	2	9	9	NUM
eurjchem-1477	248	3	]	]	PUNCT
eurjchem-1477	248	4	.	.	PUNCT
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eurjchem-1477	249	2	,	,	PUNCT
eurjchem-1477	249	3	l.	l.	PROPN
eurjchem-1477	249	4	;	;	PUNCT
eurjchem-1477	249	5	ye	ye	PROPN
eurjchem-1477	249	6	,	,	PUNCT
eurjchem-1477	249	7	d.	d.	PROPN
eurjchem-1477	249	8	;	;	PUNCT
eurjchem-1477	249	9	zhou	zhou	PROPN
eurjchem-1477	249	10	,	,	PUNCT
eurjchem-1477	249	11	y.	y.	PROPN
eurjchem-1477	249	12	;	;	PUNCT
eurjchem-1477	249	13	liu	liu	PROPN
eurjchem-1477	249	14	,	,	PUNCT
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eurjchem-1477	249	16	;	;	PUNCT
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eurjchem-1477	249	18	,	,	PUNCT
eurjchem-1477	249	19	e.	e.	PROPN
eurjchem-1477	249	20	;	;	PUNCT
eurjchem-1477	249	21	jiang	jiang	PROPN
eurjchem-1477	249	22	,	,	PUNCT
eurjchem-1477	249	23	h.	h.	PROPN
eurjchem-1477	249	24	;	;	PUNCT
eurjchem-1477	249	25	liu	liu	PROPN
eurjchem-1477	249	26	,	,	PUNCT
eurjchem-1477	249	27	h.	h.	PROPN
eurjchem-1477	249	28	j.	j.	PROPN
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eurjchem-1477	249	30	.	.	PUNCT
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eurjchem-1477	249	32	.	.	PUNCT
eurjchem-1477	250	1	2010	2010	NUM
eurjchem-1477	250	2	,	,	PUNCT
eurjchem-1477	250	3	75	75	NUM
eurjchem-1477	250	4	,	,	PUNCT
eurjchem-1477	250	5	3671‐3671	3671‐3671	NUM
eurjchem-1477	250	6	.	.	PUNCT
eurjchem-1477	251	1	[	[	X
eurjchem-1477	251	2	10	10	NUM
eurjchem-1477	251	3	]	]	PUNCT
eurjchem-1477	251	4	.	.	PUNCT
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eurjchem-1477	252	2	,	,	PUNCT
eurjchem-1477	252	3	y.	y.	PROPN
eurjchem-1477	252	4	;	;	PUNCT
eurjchem-1477	252	5	tanaka	tanaka	PROPN
eurjchem-1477	252	6	,	,	PUNCT
eurjchem-1477	252	7	t.	t.	PROPN
eurjchem-1477	252	8	;	;	PUNCT
eurjchem-1477	252	9	miwatashi	miwatashi	PROPN
eurjchem-1477	252	10	,	,	PUNCT
eurjchem-1477	252	11	s.	s.	PROPN
eurjchem-1477	252	12	;	;	PUNCT
eurjchem-1477	252	13	fujishima	fujishima	PROPN
eurjchem-1477	252	14	,	,	PUNCT
eurjchem-1477	252	15	a.	a.	NOUN
eurjchem-1477	252	16	;	;	PUNCT
eurjchem-1477	252	17	goto	goto	NOUN
eurjchem-1477	252	18	,	,	PUNCT
eurjchem-1477	252	19	g.	g.	PROPN
eurjchem-1477	252	20	j.	j.	PROPN
eurjchem-1477	252	21	chem	chem	PROPN
eurjchem-1477	252	22	.	.	PUNCT
eurjchem-1477	253	1	soc	soc	PROPN
eurjchem-1477	253	2	.	.	PUNCT
eurjchem-1477	253	3	,	,	PUNCT
eurjchem-1477	253	4	perkin	perkin	PROPN
eurjchem-1477	253	5	trans	trans	PROPN
eurjchem-1477	253	6	.	.	PROPN
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eurjchem-1477	253	8	,	,	PUNCT
eurjchem-1477	253	9	1	1	NUM
eurjchem-1477	253	10	,	,	PUNCT
eurjchem-1477	253	11	2993‐2999	2993‐2999	NUM
eurjchem-1477	253	12	.	.	PUNCT
eurjchem-1477	254	1	[	[	X
eurjchem-1477	254	2	11	11	NUM
eurjchem-1477	254	3	]	]	PUNCT
eurjchem-1477	254	4	.	.	PUNCT
eurjchem-1477	254	5	guastavino	guastavino	PROPN
eurjchem-1477	254	6	,	,	PUNCT
eurjchem-1477	254	7	j.	j.	PROPN
eurjchem-1477	254	8	f.	f.	PROPN
eurjchem-1477	254	9	;	;	PUNCT
eurjchem-1477	254	10	buden	buden	ADJ
eurjchem-1477	254	11	,	,	PUNCT
eurjchem-1477	254	12	m.	m.	PROPN
eurjchem-1477	254	13	e.	e.	PROPN
eurjchem-1477	254	14	;	;	PUNCT
eurjchem-1477	254	15	garcia	garcia	PROPN
eurjchem-1477	254	16	,	,	PUNCT
eurjchem-1477	254	17	c.	c.	PROPN
eurjchem-1477	254	18	s.	s.	PROPN
eurjchem-1477	254	19	;	;	PUNCT
eurjchem-1477	254	20	rossi	rossi	PROPN
eurjchem-1477	254	21	,	,	PUNCT
eurjchem-1477	254	22	r.	r.	PROPN
eurjchem-1477	254	23	a.	a.	PROPN
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eurjchem-1477	254	26	,	,	PUNCT
eurjchem-1477	254	27	7	7	NUM
eurjchem-1477	254	28	,	,	PUNCT
eurjchem-1477	254	29	389‐405	389‐405	NUM
eurjchem-1477	254	30	.	.	PUNCT
eurjchem-1477	255	1	[	[	X
eurjchem-1477	255	2	12	12	NUM
eurjchem-1477	255	3	]	]	PUNCT
eurjchem-1477	255	4	.	.	PUNCT
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eurjchem-1477	256	2	,	,	PUNCT
eurjchem-1477	256	3	s.	s.	PROPN
eurjchem-1477	256	4	;	;	PUNCT
eurjchem-1477	256	5	husain	husain	PROPN
eurjchem-1477	256	6	,	,	PUNCT
eurjchem-1477	256	7	s.	s.	PROPN
eurjchem-1477	256	8	m.	m.	PROPN
eurjchem-1477	256	9	;	;	PUNCT
eurjchem-1477	256	10	schepmann	schepmann	PROPN
eurjchem-1477	256	11	,	,	PUNCT
eurjchem-1477	256	12	d.	d.	PROPN
eurjchem-1477	256	13	;	;	PUNCT
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eurjchem-1477	256	15	,	,	PUNCT
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eurjchem-1477	256	17	;	;	PUNCT
eurjchem-1477	256	18	wunsch	wunsch	PROPN
eurjchem-1477	256	19	,	,	PUNCT
eurjchem-1477	256	20	b.	b.	PROPN
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eurjchem-1477	256	23	,	,	PUNCT
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eurjchem-1477	256	25	,	,	PUNCT
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eurjchem-1477	256	27	.	.	PUNCT
eurjchem-1477	257	1	[	[	X
eurjchem-1477	257	2	13	13	NUM
eurjchem-1477	257	3	]	]	PUNCT
eurjchem-1477	257	4	.	.	PUNCT
eurjchem-1477	258	1	wang	wang	PROPN
eurjchem-1477	258	2	,	,	PUNCT
eurjchem-1477	258	3	m.	m.	NOUN
eurjchem-1477	258	4	;	;	PUNCT
eurjchem-1477	258	5	gao	gao	PROPN
eurjchem-1477	258	6	,	,	PUNCT
eurjchem-1477	258	7	m.	m.	NOUN
eurjchem-1477	258	8	;	;	PUNCT
eurjchem-1477	258	9	steele	steele	PROPN
eurjchem-1477	258	10	,	,	PUNCT
eurjchem-1477	258	11	b.	b.	PROPN
eurjchem-1477	258	12	l.	l.	PROPN
eurjchem-1477	258	13	;	;	PUNCT
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eurjchem-1477	258	15	,	,	PUNCT
eurjchem-1477	258	16	b.	b.	PROPN
eurjchem-1477	258	17	e.	e.	PROPN
eurjchem-1477	258	18	;	;	PUNCT
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eurjchem-1477	258	20	,	,	PUNCT
eurjchem-1477	258	21	c.	c.	PROPN
eurjchem-1477	258	22	;	;	PUNCT
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eurjchem-1477	258	24	,	,	PUNCT
eurjchem-1477	258	25	a.	a.	PROPN
eurjchem-1477	258	26	;	;	PUNCT
eurjchem-1477	258	27	hutchins	hutchins	PROPN
eurjchem-1477	258	28	,	,	PUNCT
eurjchem-1477	258	29	g.	g.	PROPN
eurjchem-1477	258	30	d.	d.	PROPN
eurjchem-1477	258	31	;	;	PUNCT
eurjchem-1477	258	32	zheng	zheng	PROPN
eurjchem-1477	258	33	,	,	PUNCT
eurjchem-1477	258	34	q.	q.	PROPN
eurjchem-1477	258	35	h.	h.	PROPN
eurjchem-1477	258	36	;	;	PUNCT
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eurjchem-1477	259	2	.	.	PUNCT
eurjchem-1477	260	1	med	med	PROPN
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eurjchem-1477	260	4	.	.	PUNCT
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eurjchem-1477	261	2	.	.	PROPN
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eurjchem-1477	261	4	,	,	PUNCT
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eurjchem-1477	261	6	,	,	PUNCT
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eurjchem-1477	261	8	.	.	PUNCT
eurjchem-1477	262	1	[	[	X
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eurjchem-1477	262	3	]	]	PUNCT
eurjchem-1477	262	4	.	.	PUNCT
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eurjchem-1477	263	2	,	,	PUNCT
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eurjchem-1477	263	4	;	;	PUNCT
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eurjchem-1477	263	6	,	,	PUNCT
eurjchem-1477	263	7	t.	t.	PROPN
eurjchem-1477	263	8	;	;	PUNCT
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eurjchem-1477	263	10	,	,	PUNCT
eurjchem-1477	263	11	k.	k.	PROPN
eurjchem-1477	263	12	;	;	PUNCT
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eurjchem-1477	263	14	,	,	PUNCT
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eurjchem-1477	263	18	,	,	PUNCT
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eurjchem-1477	263	22	.	.	PUNCT
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eurjchem-1477	264	2	.	.	PUNCT
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eurjchem-1477	264	8	,	,	PUNCT
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eurjchem-1477	264	12	.	.	PUNCT
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eurjchem-1477	265	4	.	.	PUNCT
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eurjchem-1477	267	7	,	,	PUNCT
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eurjchem-1477	269	5	;	;	PUNCT
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eurjchem-1477	269	10	;	;	PUNCT
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eurjchem-1477	270	7	.	.	PUNCT
eurjchem-1477	271	1	[	[	X
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eurjchem-1477	271	4	.	.	PUNCT
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eurjchem-1477	272	13	;	;	PUNCT
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eurjchem-1477	273	2	.	.	PUNCT
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eurjchem-1477	274	2	,	,	PUNCT
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eurjchem-1477	274	4	,	,	PUNCT
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eurjchem-1477	275	2	,	,	PUNCT
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eurjchem-1477	276	4	.	.	PUNCT
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eurjchem-1477	277	4	;	;	PUNCT
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eurjchem-1477	277	13	;	;	PUNCT
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eurjchem-1477	277	18	;	;	PUNCT
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eurjchem-1477	277	21	d.	d.	PROPN
eurjchem-1477	277	22	l.	l.	PROPN
eurjchem-1477	277	23	j.	j.	PROPN
eurjchem-1477	277	24	org	org	PROPN
eurjchem-1477	277	25	.	.	PUNCT
eurjchem-1477	277	26	chem	chem	PROPN
eurjchem-1477	277	27	.	.	PUNCT
eurjchem-1477	278	1	2007	2007	NUM
eurjchem-1477	278	2	,	,	PUNCT
eurjchem-1477	278	3	72	72	NUM
eurjchem-1477	278	4	,	,	PUNCT
eurjchem-1477	278	5	4276‐4279	4276‐4279	NUM
eurjchem-1477	278	6	.	.	PUNCT
eurjchem-1477	279	1	[	[	X
eurjchem-1477	279	2	19	19	NUM
eurjchem-1477	279	3	]	]	PUNCT
eurjchem-1477	279	4	.	.	PUNCT
eurjchem-1477	279	5	fomenkov	fomenkov	PROPN
eurjchem-1477	279	6	,	,	PUNCT
eurjchem-1477	279	7	a.	a.	NOUN
eurjchem-1477	279	8	i.	i.	PROPN
eurjchem-1477	279	9	;	;	PUNCT
eurjchem-1477	279	10	blagodatskikh	blagodatskikh	PROPN
eurjchem-1477	279	11	,	,	PUNCT
eurjchem-1477	279	12	i.	i.	PROPN
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eurjchem-1477	279	14	;	;	PUNCT
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eurjchem-1477	279	17	i.	i.	PROPN
eurjchem-1477	279	18	i.	i.	PROPN
eurjchem-1477	279	19	;	;	PUNCT
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eurjchem-1477	279	21	,	,	PUNCT
eurjchem-1477	279	22	y.	y.	PROPN
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eurjchem-1477	280	2	,	,	PUNCT
eurjchem-1477	280	3	i.	i.	PROPN
eurjchem-1477	280	4	i.	i.	PROPN
eurjchem-1477	280	5	;	;	PUNCT
eurjchem-1477	280	6	khokhlov	khokhlov	PROPN
eurjchem-1477	280	7	,	,	PUNCT
eurjchem-1477	280	8	a.	a.	PROPN
eurjchem-1477	280	9	r.	r.	PROPN
eurjchem-1477	280	10	polym	polym	PROPN
eurjchem-1477	280	11	.	.	PUNCT
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eurjchem-1477	282	1	b+	b+	ADP
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eurjchem-1477	282	3	,	,	PUNCT
eurjchem-1477	282	4	51	51	NUM
eurjchem-1477	282	5	,	,	PUNCT
eurjchem-1477	282	6	166‐	166‐	NUM
eurjchem-1477	282	7	173	173	NUM
eurjchem-1477	282	8	.	.	PUNCT
eurjchem-1477	283	1	[	[	X
eurjchem-1477	283	2	20	20	NUM
eurjchem-1477	283	3	]	]	PUNCT
eurjchem-1477	283	4	.	.	PUNCT
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eurjchem-1477	284	2	,	,	PUNCT
eurjchem-1477	284	3	s.	s.	PROPN
eurjchem-1477	284	4	j.	j.	PROPN
eurjchem-1477	284	5	;	;	PUNCT
eurjchem-1477	284	6	lee	lee	PROPN
eurjchem-1477	284	7	,	,	PUNCT
eurjchem-1477	284	8	j.	j.	PROPN
eurjchem-1477	284	9	c.	c.	PROPN
eurjchem-1477	284	10	;	;	PUNCT
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eurjchem-1477	284	12	,	,	PUNCT
eurjchem-1477	284	13	k.	k.	PROPN
eurjchem-1477	284	14	i.	i.	PROPN
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eurjchem-1477	284	16	.	.	PUNCT
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eurjchem-1477	286	2	.	.	PUNCT
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eurjchem-1477	287	2	,	,	PUNCT
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eurjchem-1477	287	4	,	,	PUNCT
eurjchem-1477	287	5	1203‐	1203‐	NUM
eurjchem-1477	287	6	1205	1205	NUM
eurjchem-1477	287	7	.	.	PUNCT
eurjchem-1477	288	1	[	[	X
eurjchem-1477	288	2	21	21	NUM
eurjchem-1477	288	3	]	]	PUNCT
eurjchem-1477	288	4	.	.	PUNCT
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eurjchem-1477	288	6	,	,	PUNCT
eurjchem-1477	288	7	e.	e.	PROPN
eurjchem-1477	288	8	;	;	PUNCT
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eurjchem-1477	288	10	,	,	PUNCT
eurjchem-1477	288	11	m.	m.	NOUN
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eurjchem-1477	288	16	d.	d.	PROPN
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eurjchem-1477	289	4	,	,	PUNCT
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eurjchem-1477	290	4	.	.	PUNCT
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eurjchem-1477	291	2	,	,	PUNCT
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eurjchem-1477	291	5	;	;	PUNCT
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eurjchem-1477	291	7	,	,	PUNCT
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eurjchem-1477	291	10	;	;	PUNCT
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eurjchem-1477	291	12	,	,	PUNCT
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eurjchem-1477	291	16	.	.	PUNCT
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eurjchem-1477	292	2	.	.	PUNCT
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eurjchem-1477	293	2	,	,	PUNCT
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eurjchem-1477	293	4	,	,	PUNCT
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eurjchem-1477	293	6	.	.	PUNCT
eurjchem-1477	294	1	[	[	X
eurjchem-1477	294	2	23	23	NUM
eurjchem-1477	294	3	]	]	PUNCT
eurjchem-1477	294	4	.	.	PUNCT
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eurjchem-1477	295	2	,	,	PUNCT
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eurjchem-1477	295	4	;	;	PUNCT
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eurjchem-1477	295	10	,	,	PUNCT
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eurjchem-1477	297	2	,	,	PUNCT
eurjchem-1477	297	3	l.	l.	PROPN
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eurjchem-1477	297	5	;	;	PUNCT
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eurjchem-1477	297	7	,	,	PUNCT
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eurjchem-1477	297	9	r.	r.	PROPN
eurjchem-1477	297	10	j.	j.	PROPN
eurjchem-1477	297	11	org	org	PROPN
eurjchem-1477	297	12	.	.	PUNCT
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eurjchem-1477	298	2	,	,	PUNCT
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eurjchem-1477	298	4	,	,	PUNCT
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eurjchem-1477	298	6	.	.	PUNCT
eurjchem-1477	299	1	[	[	X
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eurjchem-1477	299	4	.	.	PUNCT
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eurjchem-1477	300	2	,	,	PUNCT
eurjchem-1477	300	3	s.	s.	PROPN
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eurjchem-1477	300	5	;	;	PUNCT
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eurjchem-1477	300	7	,	,	PUNCT
eurjchem-1477	300	8	s.	s.	PROPN
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eurjchem-1477	300	10	;	;	PUNCT
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eurjchem-1477	300	20	;	;	PUNCT
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eurjchem-1477	300	22	,	,	PUNCT
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eurjchem-1477	301	1	org	org	PROPN
eurjchem-1477	301	2	.	.	PUNCT
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eurjchem-1477	301	4	.	.	PUNCT
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eurjchem-1477	302	2	,	,	PUNCT
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eurjchem-1477	302	4	,	,	PUNCT
eurjchem-1477	302	5	526‐529	526‐529	NUM
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eurjchem-1477	303	1	[	[	X
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eurjchem-1477	303	4	.	.	PUNCT
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eurjchem-1477	304	5	;	;	PUNCT
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eurjchem-1477	304	7	,	,	PUNCT
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eurjchem-1477	304	10	;	;	PUNCT
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eurjchem-1477	305	1	j.	j.	PROPN
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eurjchem-1477	306	2	,	,	PUNCT
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