id	sid	tid	token	lemma	pos
eurjchem-1541	1	1	untitled	untitle	VERB
eurjchem-1541	1	2	european	european	PROPN
eurjchem-1541	1	3	journal	journal	PROPN
eurjchem-1541	1	4	of	of	ADP
eurjchem-1541	1	5	chemistry	chemistry	NOUN
eurjchem-1541	1	6	8	8	NUM
eurjchem-1541	1	7	(	(	PUNCT
eurjchem-1541	1	8	2	2	NUM
eurjchem-1541	1	9	)	)	PUNCT
eurjchem-1541	1	10	(	(	PUNCT
eurjchem-1541	1	11	2017	2017	NUM
eurjchem-1541	1	12	)	)	PUNCT
eurjchem-1541	1	13	105‐108	105‐108	PROPN
eurjchem-1541	1	14	european	european	PROPN
eurjchem-1541	1	15	journal	journal	PROPN
eurjchem-1541	1	16	of	of	ADP
eurjchem-1541	1	17	chemistry	chemistry	NOUN
eurjchem-1541	1	18	issn	issn	PROPN
eurjchem-1541	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-1541	1	20	(	(	PUNCT
eurjchem-1541	1	21	print	print	NOUN
eurjchem-1541	1	22	)	)	PUNCT
eurjchem-1541	1	23	/	/	SYM
eurjchem-1541	1	24	issn	issn	PROPN
eurjchem-1541	1	25	2153‐2257	2153‐2257	NUM
eurjchem-1541	1	26	(	(	PUNCT
eurjchem-1541	1	27	online	online	ADJ
eurjchem-1541	1	28	)	)	PUNCT
eurjchem-1541	1	29			NOUN
eurjchem-1541	1	30	2017	2017	NUM
eurjchem-1541	1	31	atlanta	atlanta	PROPN
eurjchem-1541	1	32	publishing	publishing	PROPN
eurjchem-1541	1	33	house	house	PROPN
eurjchem-1541	1	34	llc	llc	PROPN
eurjchem-1541	1	35	‐	‐	PUNCT
eurjchem-1541	1	36	all	all	DET
eurjchem-1541	1	37	rights	right	NOUN
eurjchem-1541	1	38	reserved	reserve	VERB
eurjchem-1541	1	39	‐	‐	NOUN
eurjchem-1541	1	40	printed	print	VERB
eurjchem-1541	1	41	in	in	ADP
eurjchem-1541	1	42	the	the	DET
eurjchem-1541	1	43	usa	usa	PROPN
eurjchem-1541	1	44	http://dx.doi.org/10.5155/eurjchem.8.2.105-108.1541	http://dx.doi.org/10.5155/eurjchem.8.2.105-108.1541	PROPN
eurjchem-1541	1	45	european	european	PROPN
eurjchem-1541	1	46	journal	journal	PROPN
eurjchem-1541	1	47	of	of	ADP
eurjchem-1541	1	48	chemistry	chemistry	PROPN
eurjchem-1541	1	49	journal	journal	PROPN
eurjchem-1541	1	50	webpage	webpage	NOUN
eurjchem-1541	1	51	:	:	PUNCT
eurjchem-1541	1	52	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1541	1	53	synthesis	synthesis	NOUN
eurjchem-1541	1	54	,	,	PUNCT
eurjchem-1541	1	55	and	and	CCONJ
eurjchem-1541	1	56	evaluation	evaluation	NOUN
eurjchem-1541	1	57	of	of	ADP
eurjchem-1541	1	58	α‐amylase	α‐amylase	NUM
eurjchem-1541	1	59	and	and	CCONJ
eurjchem-1541	1	60	α‐glucosidase	α‐glucosidase	X
eurjchem-1541	1	61	inhibitory	inhibitory	ADJ
eurjchem-1541	1	62	potential	potential	NOUN
eurjchem-1541	1	63	of	of	ADP
eurjchem-1541	1	64	new	new	ADJ
eurjchem-1541	1	65	pyrazolo[3,4‐d]pyrimidine	pyrazolo[3,4‐d]pyrimidine	NOUN
eurjchem-1541	1	66	derivatives	derivative	NOUN
eurjchem-1541	1	67	mohammed	mohammed	PROPN
eurjchem-1541	1	68	el‐fal	el‐fal	PROPN
eurjchem-1541	1	69	1,2	1,2	NUM
eurjchem-1541	1	70	,	,	PUNCT
eurjchem-1541	1	71	karima	karima	PROPN
eurjchem-1541	1	72	sayah	sayah	PROPN
eurjchem-1541	1	73	3	3	NUM
eurjchem-1541	1	74	,	,	PUNCT
eurjchem-1541	1	75	ilias	ilias	PROPN
eurjchem-1541	1	76	marmouzi	marmouzi	PROPN
eurjchem-1541	1	77	3	3	NUM
eurjchem-1541	1	78	,	,	PUNCT
eurjchem-1541	1	79	my	my	PRON
eurjchem-1541	1	80	el	el	PROPN
eurjchem-1541	1	81	abbes	abbe	NOUN
eurjchem-1541	1	82	faouzi	faouzi	VERB
eurjchem-1541	1	83	3	3	NUM
eurjchem-1541	1	84	,	,	PUNCT
eurjchem-1541	1	85	m'hammed	m'hammed	PROPN
eurjchem-1541	1	86	ansar	ansar	PROPN
eurjchem-1541	1	87	1	1	NUM
eurjchem-1541	1	88	,	,	PUNCT
eurjchem-1541	1	89	jamal	jamal	PROPN
eurjchem-1541	1	90	taoufik	taoufik	VERB
eurjchem-1541	1	91	1	1	NUM
eurjchem-1541	1	92	,	,	PUNCT
eurjchem-1541	1	93	el	el	PROPN
eurjchem-1541	1	94	mokhtar	mokhtar	PROPN
eurjchem-1541	1	95	essassi	essassi	PROPN
eurjchem-1541	1	96	2	2	NUM
eurjchem-1541	1	97	and	and	CCONJ
eurjchem-1541	1	98	youssef	youssef	PROPN
eurjchem-1541	1	99	ramli	ramli	PROPN
eurjchem-1541	1	100	1	1	NUM
eurjchem-1541	1	101	,	,	PUNCT
eurjchem-1541	1	102	*	*	PUNCT
eurjchem-1541	1	103	1	1	NUM
eurjchem-1541	1	104	medicinal	medicinal	ADJ
eurjchem-1541	1	105	chemistry	chemistry	NOUN
eurjchem-1541	1	106	laboratory	laboratory	NOUN
eurjchem-1541	1	107	,	,	PUNCT
eurjchem-1541	1	108	faculty	faculty	NOUN
eurjchem-1541	1	109	of	of	ADP
eurjchem-1541	1	110	medicine	medicine	NOUN
eurjchem-1541	1	111	and	and	CCONJ
eurjchem-1541	1	112	pharmacy	pharmacy	NOUN
eurjchem-1541	1	113	,	,	PUNCT
eurjchem-1541	1	114	mohammed	mohammed	PROPN
eurjchem-1541	1	115	v	v	PROPN
eurjchem-1541	1	116	university	university	PROPN
eurjchem-1541	1	117	,	,	PUNCT
eurjchem-1541	1	118	10170	10170	NUM
eurjchem-1541	1	119	,	,	PUNCT
eurjchem-1541	1	120	rabat	rabat	NOUN
eurjchem-1541	1	121	,	,	PUNCT
eurjchem-1541	1	122	morocco	morocco	PROPN
eurjchem-1541	1	123	2	2	NUM
eurjchem-1541	1	124	laboratory	laboratory	NOUN
eurjchem-1541	1	125	of	of	ADP
eurjchem-1541	1	126	organic	organic	ADJ
eurjchem-1541	1	127	heterocyclic	heterocyclic	ADJ
eurjchem-1541	1	128	chemistry	chemistry	NOUN
eurjchem-1541	1	129	urac	urac	NOUN
eurjchem-1541	1	130	21	21	NUM
eurjchem-1541	1	131	,	,	PUNCT
eurjchem-1541	1	132	faculty	faculty	NOUN
eurjchem-1541	1	133	of	of	ADP
eurjchem-1541	1	134	sciences	science	NOUN
eurjchem-1541	1	135	,	,	PUNCT
eurjchem-1541	1	136	mohammed	mohammed	PROPN
eurjchem-1541	1	137	v	v	PROPN
eurjchem-1541	1	138	university	university	PROPN
eurjchem-1541	1	139	,	,	PUNCT
eurjchem-1541	1	140	10170	10170	NUM
eurjchem-1541	1	141	,	,	PUNCT
eurjchem-1541	1	142	rabat	rabat	NOUN
eurjchem-1541	1	143	,	,	PUNCT
eurjchem-1541	1	144	morocco	morocco	PROPN
eurjchem-1541	1	145	3	3	NUM
eurjchem-1541	1	146	laboratories	laboratory	NOUN
eurjchem-1541	1	147	of	of	ADP
eurjchem-1541	1	148	pharmacology	pharmacology	NOUN
eurjchem-1541	1	149	and	and	CCONJ
eurjchem-1541	1	150	toxicology	toxicology	NOUN
eurjchem-1541	1	151	,	,	PUNCT
eurjchem-1541	1	152	faculty	faculty	NOUN
eurjchem-1541	1	153	of	of	ADP
eurjchem-1541	1	154	medicine	medicine	NOUN
eurjchem-1541	1	155	and	and	CCONJ
eurjchem-1541	1	156	pharmacy	pharmacy	NOUN
eurjchem-1541	1	157	,	,	PUNCT
eurjchem-1541	1	158	mohammed	mohammed	PROPN
eurjchem-1541	1	159	v	v	PROPN
eurjchem-1541	1	160	university	university	PROPN
eurjchem-1541	1	161	,	,	PUNCT
eurjchem-1541	1	162	10170	10170	NUM
eurjchem-1541	1	163	,	,	PUNCT
eurjchem-1541	1	164	rabat	rabat	NOUN
eurjchem-1541	1	165	,	,	PUNCT
eurjchem-1541	1	166	morocco	morocco	PROPN
eurjchem-1541	1	167	*	*	PUNCT
eurjchem-1541	1	168	corresponding	correspond	VERB
eurjchem-1541	1	169	author	author	NOUN
eurjchem-1541	1	170	at	at	ADP
eurjchem-1541	1	171	:	:	PUNCT
eurjchem-1541	1	172	medicinal	medicinal	ADJ
eurjchem-1541	1	173	chemistry	chemistry	NOUN
eurjchem-1541	1	174	laboratory	laboratory	NOUN
eurjchem-1541	1	175	,	,	PUNCT
eurjchem-1541	1	176	faculty	faculty	NOUN
eurjchem-1541	1	177	of	of	ADP
eurjchem-1541	1	178	medicine	medicine	NOUN
eurjchem-1541	1	179	and	and	CCONJ
eurjchem-1541	1	180	pharmacy	pharmacy	NOUN
eurjchem-1541	1	181	,	,	PUNCT
eurjchem-1541	1	182	mohammed	mohammed	PROPN
eurjchem-1541	1	183	v	v	PROPN
eurjchem-1541	1	184	university	university	PROPN
eurjchem-1541	1	185	,	,	PUNCT
eurjchem-1541	1	186	10170	10170	NUM
eurjchem-1541	1	187	,	,	PUNCT
eurjchem-1541	1	188	rabat	rabat	NOUN
eurjchem-1541	1	189	,	,	PUNCT
eurjchem-1541	1	190	morocco	morocco	PROPN
eurjchem-1541	1	191	.	.	PUNCT
eurjchem-1541	2	1	tel	tel	PROPN
eurjchem-1541	2	2	.	.	PUNCT
eurjchem-1541	2	3	:	:	PUNCT
eurjchem-1541	3	1	+212.6.70515279	+212.6.70515279	PROPN
eurjchem-1541	3	2	.	.	PUNCT
eurjchem-1541	3	3	fax	fax	NOUN
eurjchem-1541	3	4	:	:	PUNCT
eurjchem-1541	3	5	+212.5.37773701	+212.5.37773701	PROPN
eurjchem-1541	3	6	.	.	PUNCT
eurjchem-1541	3	7	e‐mail	e‐mail	PUNCT
eurjchem-1541	4	1	address	address	NOUN
eurjchem-1541	4	2	:	:	PUNCT
eurjchem-1541	4	3	yramli76@yahoo.fr	yramli76@yahoo.fr	PROPN
eurjchem-1541	4	4	(	(	PUNCT
eurjchem-1541	4	5	y.	y.	PROPN
eurjchem-1541	4	6	ramli	ramli	PROPN
eurjchem-1541	4	7	)	)	PUNCT
eurjchem-1541	4	8	.	.	PUNCT
eurjchem-1541	5	1	article	article	NOUN
eurjchem-1541	5	2	information	information	PROPN
eurjchem-1541	5	3	abstract	abstract	ADJ
eurjchem-1541	5	4	doi	doi	PROPN
eurjchem-1541	5	5	:	:	PUNCT
eurjchem-1541	5	6	 	 	SPACE
eurjchem-1541	5	7	10.5155	10.5155	NUM
eurjchem-1541	5	8	/	/	SYM
eurjchem-1541	5	9	eurjchem.8.2.105	eurjchem.8.2.105	NOUN
eurjchem-1541	5	10	-	-	PUNCT
eurjchem-1541	5	11	108.1541	108.1541	NUM
eurjchem-1541	5	12	received	receive	VERB
eurjchem-1541	5	13	:	:	PUNCT
eurjchem-1541	5	14	31	31	NUM
eurjchem-1541	5	15	december	december	PROPN
eurjchem-1541	5	16	2016	2016	NUM
eurjchem-1541	5	17	received	receive	VERB
eurjchem-1541	5	18	in	in	ADP
eurjchem-1541	5	19	revised	revise	VERB
eurjchem-1541	5	20	form	form	NOUN
eurjchem-1541	5	21	:	:	PUNCT
eurjchem-1541	5	22	20	20	NUM
eurjchem-1541	5	23	january	january	NOUN
eurjchem-1541	5	24	2017	2017	NUM
eurjchem-1541	5	25	accepted	accept	VERB
eurjchem-1541	5	26	:	:	PUNCT
eurjchem-1541	5	27	11	11	NUM
eurjchem-1541	5	28	february	february	NOUN
eurjchem-1541	5	29	2017	2017	NUM
eurjchem-1541	5	30	published	publish	VERB
eurjchem-1541	5	31	online	online	ADV
eurjchem-1541	5	32	:	:	PUNCT
eurjchem-1541	5	33	30	30	NUM
eurjchem-1541	5	34	june	june	PROPN
eurjchem-1541	5	35	2017	2017	NUM
eurjchem-1541	5	36	printed	print	VERB
eurjchem-1541	5	37	:	:	PUNCT
eurjchem-1541	5	38	30	30	NUM
eurjchem-1541	5	39	june	june	PROPN
eurjchem-1541	5	40	2017	2017	NUM
eurjchem-1541	5	41	  	  	SPACE
eurjchem-1541	5	42	a	a	DET
eurjchem-1541	5	43	series	series	NOUN
eurjchem-1541	5	44	of	of	ADP
eurjchem-1541	5	45	new	new	ADJ
eurjchem-1541	5	46	pyrazolo[3,4‐d]pyrimidine	pyrazolo[3,4‐d]pyrimidine	NOUN
eurjchem-1541	5	47	compounds	compound	NOUN
eurjchem-1541	5	48	were	be	AUX
eurjchem-1541	5	49	synthesized	synthesize	VERB
eurjchem-1541	5	50	in	in	ADP
eurjchem-1541	5	51	excellent	excellent	ADJ
eurjchem-1541	5	52	yields	yield	NOUN
eurjchem-1541	5	53	via	via	ADP
eurjchem-1541	5	54	sulfuration	sulfuration	NOUN
eurjchem-1541	5	55	and	and	CCONJ
eurjchem-1541	5	56	1,3‐dipolar	1,3‐dipolar	NUM
eurjchem-1541	5	57	cycloaddition	cycloaddition	NOUN
eurjchem-1541	5	58	and	and	CCONJ
eurjchem-1541	5	59	confirmed	confirm	VERB
eurjchem-1541	5	60	by	by	ADP
eurjchem-1541	5	61	ms	ms	PROPN
eurjchem-1541	5	62	,	,	PUNCT
eurjchem-1541	5	63	ft‐ir	ft‐ir	NOUN
eurjchem-1541	5	64	and	and	CCONJ
eurjchem-1541	5	65	nmr	nmr	NOUN
eurjchem-1541	5	66	techniques	technique	NOUN
eurjchem-1541	5	67	.	.	PUNCT
eurjchem-1541	6	1	all	all	DET
eurjchem-1541	6	2	the	the	DET
eurjchem-1541	6	3	prepared	prepare	VERB
eurjchem-1541	6	4	compounds	compound	NOUN
eurjchem-1541	6	5	were	be	AUX
eurjchem-1541	6	6	screened	screen	VERB
eurjchem-1541	6	7	in	in	ADP
eurjchem-1541	6	8	vitro	vitro	X
eurjchem-1541	6	9	for	for	ADP
eurjchem-1541	6	10	their	their	PRON
eurjchem-1541	6	11	α‐amylase	α‐amylase	NUM
eurjchem-1541	6	12	and	and	CCONJ
eurjchem-1541	6	13	α‐	α‐	NUM
eurjchem-1541	6	14	glucosidase	glucosidase	ADJ
eurjchem-1541	6	15	inhibitory	inhibitory	ADJ
eurjchem-1541	6	16	activities	activity	NOUN
eurjchem-1541	6	17	.	.	PUNCT
eurjchem-1541	7	1	preliminary	preliminary	ADJ
eurjchem-1541	7	2	results	result	NOUN
eurjchem-1541	7	3	indicated	indicate	VERB
eurjchem-1541	7	4	that	that	SCONJ
eurjchem-1541	7	5	some	some	DET
eurjchem-1541	7	6	target	target	NOUN
eurjchem-1541	7	7	compounds	compound	NOUN
eurjchem-1541	7	8	exhibited	exhibit	VERB
eurjchem-1541	7	9	promising	promise	VERB
eurjchem-1541	7	10	α‐amylase	α‐amylase	NUM
eurjchem-1541	7	11	and	and	CCONJ
eurjchem-1541	7	12	α‐glucosidase	α‐glucosidase	X
eurjchem-1541	7	13	inhibitory	inhibitory	ADJ
eurjchem-1541	7	14	activity	activity	NOUN
eurjchem-1541	7	15	potency	potency	NOUN
eurjchem-1541	7	16	.	.	PUNCT
eurjchem-1541	8	1	among	among	ADP
eurjchem-1541	8	2	the	the	DET
eurjchem-1541	8	3	tested	test	VERB
eurjchem-1541	8	4	products	product	NOUN
eurjchem-1541	8	5	,	,	PUNCT
eurjchem-1541	8	6	the	the	DET
eurjchem-1541	8	7	cycloadduct	cycloadduct	NOUN
eurjchem-1541	8	8	f	f	PROPN
eurjchem-1541	8	9	was	be	AUX
eurjchem-1541	8	10	found	find	VERB
eurjchem-1541	8	11	most	most	ADV
eurjchem-1541	8	12	active	active	ADJ
eurjchem-1541	8	13	inhibitor	inhibitor	NOUN
eurjchem-1541	8	14	(	(	PUNCT
eurjchem-1541	8	15	ic50	ic50	PROPN
eurjchem-1541	8	16	=	=	PUNCT
eurjchem-1541	8	17	134.30	134.30	NUM
eurjchem-1541	8	18	μm	μm	NUM
eurjchem-1541	8	19	)	)	PUNCT
eurjchem-1541	8	20	for	for	ADP
eurjchem-1541	8	21	α‐	α‐	NUM
eurjchem-1541	8	22	amylase	amylase	NOUN
eurjchem-1541	8	23	,	,	PUNCT
eurjchem-1541	8	24	and	and	CCONJ
eurjchem-1541	8	25	the	the	DET
eurjchem-1541	8	26	sulphur	sulphur	NOUN
eurjchem-1541	8	27	product	product	NOUN
eurjchem-1541	8	28	b	b	PROPN
eurjchem-1541	8	29	is	be	AUX
eurjchem-1541	8	30	the	the	DET
eurjchem-1541	8	31	most	most	ADV
eurjchem-1541	8	32	active	active	ADJ
eurjchem-1541	8	33	inhibitor	inhibitor	NOUN
eurjchem-1541	8	34	(	(	PUNCT
eurjchem-1541	8	35	ic50	ic50	PROPN
eurjchem-1541	8	36	=	=	PROPN
eurjchem-1541	8	37	16.37	16.37	NUM
eurjchem-1541	8	38	μm	μm	NUM
eurjchem-1541	8	39	)	)	PUNCT
eurjchem-1541	8	40	for	for	ADP
eurjchem-1541	8	41	α‐	α‐	PROPN
eurjchem-1541	8	42	glucosidase	glucosidase	NOUN
eurjchem-1541	8	43	.	.	PUNCT
eurjchem-1541	9	1	keywords	keyword	NOUN
eurjchem-1541	9	2	α‐amylase	α‐amylase	NUM
eurjchem-1541	9	3	ic50	ic50	PROPN
eurjchem-1541	9	4	values	value	NOUN
eurjchem-1541	9	5	α‐glucosidase	α‐glucosidase	PUNCT
eurjchem-1541	9	6	inhibitory	inhibitory	ADJ
eurjchem-1541	9	7	activity	activity	NOUN
eurjchem-1541	9	8	1,3‐dipolarcyclo	1,3‐dipolarcyclo	NUM
eurjchem-1541	9	9	addition	addition	NOUN
eurjchem-1541	9	10	pyrazolo[3,4‐d]pyrimidine	pyrazolo[3,4‐d]pyrimidine	NOUN
eurjchem-1541	9	11	cite	cite	VERB
eurjchem-1541	9	12	this	this	PRON
eurjchem-1541	9	13	:	:	PUNCT
eurjchem-1541	9	14	eur	eur	PROPN
eurjchem-1541	9	15	.	.	PUNCT
eurjchem-1541	10	1	j.	j.	PROPN
eurjchem-1541	10	2	chem	chem	PROPN
eurjchem-1541	10	3	.	.	PUNCT
eurjchem-1541	11	1	2017	2017	NUM
eurjchem-1541	11	2	,	,	PUNCT
eurjchem-1541	11	3	8(2	8(2	NUM
eurjchem-1541	11	4	)	)	PUNCT
eurjchem-1541	11	5	,	,	PUNCT
eurjchem-1541	11	6	105‐108	105‐108	PROPN
eurjchem-1541	11	7	1	1	NUM
eurjchem-1541	11	8	.	.	PUNCT
eurjchem-1541	12	1	introduction	introduction	NOUN
eurjchem-1541	12	2	diabetes	diabetes	NOUN
eurjchem-1541	12	3	affects	affect	VERB
eurjchem-1541	12	4	415	415	NUM
eurjchem-1541	12	5	million	million	NUM
eurjchem-1541	12	6	people	people	NOUN
eurjchem-1541	12	7	worldwide	worldwide	ADV
eurjchem-1541	12	8	and	and	CCONJ
eurjchem-1541	12	9	this	this	DET
eurjchem-1541	12	10	number	number	NOUN
eurjchem-1541	12	11	is	be	AUX
eurjchem-1541	12	12	projected	project	VERB
eurjchem-1541	12	13	to	to	PART
eurjchem-1541	12	14	rise	rise	VERB
eurjchem-1541	12	15	to	to	ADP
eurjchem-1541	12	16	642	642	NUM
eurjchem-1541	12	17	million	million	NUM
eurjchem-1541	12	18	by	by	ADP
eurjchem-1541	12	19	2040	2040	NUM
eurjchem-1541	13	1	[	[	X
eurjchem-1541	13	2	1	1	NUM
eurjchem-1541	13	3	]	]	PUNCT
eurjchem-1541	13	4	.	.	PUNCT
eurjchem-1541	14	1	it	it	PRON
eurjchem-1541	14	2	is	be	AUX
eurjchem-1541	14	3	partly	partly	ADV
eurjchem-1541	14	4	caused	cause	VERB
eurjchem-1541	14	5	by	by	ADP
eurjchem-1541	14	6	the	the	DET
eurjchem-1541	14	7	excessive	excessive	ADJ
eurjchem-1541	14	8	presence	presence	NOUN
eurjchem-1541	14	9	of	of	ADP
eurjchem-1541	14	10	carbohydrates	carbohydrate	NOUN
eurjchem-1541	14	11	in	in	ADP
eurjchem-1541	14	12	the	the	DET
eurjchem-1541	14	13	diet	diet	NOUN
eurjchem-1541	14	14	.	.	PUNCT
eurjchem-1541	15	1	starch	starch	NOUN
eurjchem-1541	15	2	digestion	digestion	NOUN
eurjchem-1541	15	3	in	in	ADP
eurjchem-1541	15	4	mammals	mammal	NOUN
eurjchem-1541	15	5	is	be	AUX
eurjchem-1541	15	6	mainly	mainly	ADV
eurjchem-1541	15	7	carried	carry	VERB
eurjchem-1541	15	8	out	out	ADP
eurjchem-1541	15	9	by	by	ADP
eurjchem-1541	15	10	α‐amylase	α‐amylase	NUM
eurjchem-1541	15	11	and	and	CCONJ
eurjchem-1541	15	12	α‐glucosidase	α‐glucosidase	X
eurjchem-1541	16	1	[	[	X
eurjchem-1541	16	2	2	2	NUM
eurjchem-1541	16	3	]	]	PUNCT
eurjchem-1541	16	4	.	.	PUNCT
eurjchem-1541	17	1	type	type	NOUN
eurjchem-1541	17	2	2	2	NUM
eurjchem-1541	17	3	diabetes	diabetes	NOUN
eurjchem-1541	17	4	mellitus	mellitus	NOUN
eurjchem-1541	17	5	(	(	PUNCT
eurjchem-1541	17	6	t2	t2	NOUN
eurjchem-1541	17	7	dm	dm	PROPN
eurjchem-1541	17	8	)	)	PUNCT
eurjchem-1541	17	9	is	be	AUX
eurjchem-1541	17	10	a	a	DET
eurjchem-1541	17	11	complex	complex	ADJ
eurjchem-1541	17	12	and	and	CCONJ
eurjchem-1541	17	13	chronic	chronic	ADJ
eurjchem-1541	17	14	metabolic	metabolic	NOUN
eurjchem-1541	17	15	disease	disease	NOUN
eurjchem-1541	17	16	due	due	ADP
eurjchem-1541	17	17	to	to	ADP
eurjchem-1541	17	18	insulin‐resistance	insulin‐resistance	NOUN
eurjchem-1541	17	19	in	in	ADP
eurjchem-1541	17	20	body	body	NOUN
eurjchem-1541	17	21	tissue	tissue	NOUN
eurjchem-1541	18	1	[	[	X
eurjchem-1541	18	2	3	3	NUM
eurjchem-1541	18	3	]	]	PUNCT
eurjchem-1541	18	4	.	.	PUNCT
eurjchem-1541	19	1	the	the	DET
eurjchem-1541	19	2	insulin	insulin	NOUN
eurjchem-1541	19	3	resistance	resistance	NOUN
eurjchem-1541	19	4	leads	lead	VERB
eurjchem-1541	19	5	to	to	ADP
eurjchem-1541	19	6	hyperglycemia	hyperglycemia	NOUN
eurjchem-1541	19	7	,	,	PUNCT
eurjchem-1541	19	8	which	which	PRON
eurjchem-1541	19	9	can	can	AUX
eurjchem-1541	19	10	damage	damage	VERB
eurjchem-1541	19	11	many	many	ADJ
eurjchem-1541	19	12	of	of	ADP
eurjchem-1541	19	13	organs	organ	NOUN
eurjchem-1541	19	14	[	[	X
eurjchem-1541	19	15	4	4	NUM
eurjchem-1541	19	16	]	]	PUNCT
eurjchem-1541	19	17	.	.	PUNCT
eurjchem-1541	20	1	one	one	NUM
eurjchem-1541	20	2	of	of	ADP
eurjchem-1541	20	3	the	the	DET
eurjchem-1541	20	4	therapeutic	therapeutic	ADJ
eurjchem-1541	20	5	approaches	approach	NOUN
eurjchem-1541	20	6	for	for	ADP
eurjchem-1541	20	7	alleviating	alleviate	VERB
eurjchem-1541	20	8	t2	t2	NOUN
eurjchem-1541	20	9	dm	dm	NOUN
eurjchem-1541	20	10	is	be	AUX
eurjchem-1541	20	11	to	to	PART
eurjchem-1541	20	12	suppress	suppress	VERB
eurjchem-1541	20	13	the	the	DET
eurjchem-1541	20	14	glucose	glucose	NOUN
eurjchem-1541	20	15	absorption	absorption	NOUN
eurjchem-1541	20	16	from	from	ADP
eurjchem-1541	20	17	the	the	DET
eurjchem-1541	20	18	intestine	intestine	NOUN
eurjchem-1541	20	19	through	through	ADP
eurjchem-1541	20	20	the	the	DET
eurjchem-1541	20	21	inhibition	inhibition	NOUN
eurjchem-1541	20	22	of	of	ADP
eurjchem-1541	20	23	carbohydrate	carbohydrate	NOUN
eurjchem-1541	20	24	hydrolyzing	hydrolyze	VERB
eurjchem-1541	20	25	enzymes	enzyme	NOUN
eurjchem-1541	20	26	such	such	ADJ
eurjchem-1541	20	27	as	as	ADP
eurjchem-1541	20	28	α‐amylase	α‐amylase	NUM
eurjchem-1541	20	29	and	and	CCONJ
eurjchem-1541	20	30	α‐glucosidase	α‐glucosidase	X
eurjchem-1541	21	1	[	[	X
eurjchem-1541	21	2	5	5	NUM
eurjchem-1541	21	3	]	]	PUNCT
eurjchem-1541	21	4	.	.	PUNCT
eurjchem-1541	21	5	α‐amylase	α‐amylase	PUNCT
eurjchem-1541	21	6	,	,	PUNCT
eurjchem-1541	21	7	which	which	PRON
eurjchem-1541	21	8	is	be	AUX
eurjchem-1541	21	9	mainly	mainly	ADV
eurjchem-1541	21	10	found	find	VERB
eurjchem-1541	21	11	in	in	ADP
eurjchem-1541	21	12	the	the	DET
eurjchem-1541	21	13	saliva	saliva	NOUN
eurjchem-1541	21	14	and	and	CCONJ
eurjchem-1541	21	15	pancreatic	pancreatic	ADJ
eurjchem-1541	21	16	juice	juice	NOUN
eurjchem-1541	21	17	,	,	PUNCT
eurjchem-1541	21	18	breaks	break	VERB
eurjchem-1541	21	19	down	down	ADP
eurjchem-1541	21	20	large	large	ADJ
eurjchem-1541	21	21	insoluble	insoluble	ADJ
eurjchem-1541	21	22	carbohydrate	carbohydrate	NOUN
eurjchem-1541	21	23	molecules	molecule	NOUN
eurjchem-1541	21	24	into	into	ADP
eurjchem-1541	21	25	oligosaccharides	oligosaccharide	NOUN
eurjchem-1541	21	26	,	,	PUNCT
eurjchem-1541	21	27	and	and	CCONJ
eurjchem-1541	21	28	α‐glucosidase	α‐glucosidase	PUNCT
eurjchem-1541	21	29	,	,	PUNCT
eurjchem-1541	21	30	which	which	PRON
eurjchem-1541	21	31	is	be	AUX
eurjchem-1541	21	32	in	in	ADP
eurjchem-1541	21	33	the	the	DET
eurjchem-1541	21	34	brush	brush	NOUN
eurjchem-1541	21	35	border	border	NOUN
eurjchem-1541	21	36	in	in	ADP
eurjchem-1541	21	37	the	the	DET
eurjchem-1541	21	38	small	small	ADJ
eurjchem-1541	21	39	intestine	intestine	NOUN
eurjchem-1541	21	40	,	,	PUNCT
eurjchem-1541	21	41	is	be	AUX
eurjchem-1541	21	42	involved	involve	VERB
eurjchem-1541	21	43	in	in	ADP
eurjchem-1541	21	44	the	the	DET
eurjchem-1541	21	45	breakdown	breakdown	NOUN
eurjchem-1541	21	46	of	of	ADP
eurjchem-1541	21	47	disaccharides	disaccharide	NOUN
eurjchem-1541	21	48	to	to	ADP
eurjchem-1541	21	49	glucose	glucose	NOUN
eurjchem-1541	21	50	[	[	X
eurjchem-1541	21	51	6	6	NUM
eurjchem-1541	21	52	]	]	PUNCT
eurjchem-1541	21	53	.	.	PUNCT
eurjchem-1541	22	1	inhibitors	inhibitor	NOUN
eurjchem-1541	22	2	of	of	ADP
eurjchem-1541	22	3	α‐amylase	α‐amylase	NUM
eurjchem-1541	22	4	and	and	CCONJ
eurjchem-1541	22	5	α‐	α‐	NUM
eurjchem-1541	22	6	glucosidase	glucosidase	NOUN
eurjchem-1541	22	7	can	can	AUX
eurjchem-1541	22	8	delay	delay	VERB
eurjchem-1541	22	9	the	the	DET
eurjchem-1541	22	10	digestion	digestion	NOUN
eurjchem-1541	22	11	of	of	ADP
eurjchem-1541	22	12	carbohydrates	carbohydrate	NOUN
eurjchem-1541	22	13	in	in	ADP
eurjchem-1541	22	14	the	the	DET
eurjchem-1541	22	15	small	small	ADJ
eurjchem-1541	22	16	intestine	intestine	NOUN
eurjchem-1541	22	17	and	and	CCONJ
eurjchem-1541	22	18	reduce	reduce	VERB
eurjchem-1541	22	19	the	the	DET
eurjchem-1541	22	20	level	level	NOUN
eurjchem-1541	22	21	of	of	ADP
eurjchem-1541	22	22	postprandial	postprandial	ADJ
eurjchem-1541	22	23	blood	blood	NOUN
eurjchem-1541	22	24	glucose	glucose	NOUN
eurjchem-1541	22	25	[	[	X
eurjchem-1541	22	26	7	7	NUM
eurjchem-1541	22	27	]	]	PUNCT
eurjchem-1541	22	28	.	.	PUNCT
eurjchem-1541	23	1	many	many	ADJ
eurjchem-1541	23	2	studies	study	NOUN
eurjchem-1541	23	3	have	have	AUX
eurjchem-1541	23	4	searched	search	VERB
eurjchem-1541	23	5	for	for	ADP
eurjchem-1541	23	6	safe	safe	ADJ
eurjchem-1541	23	7	and	and	CCONJ
eurjchem-1541	23	8	effective	effective	ADJ
eurjchem-1541	23	9	inhibitors	inhibitor	NOUN
eurjchem-1541	23	10	of	of	ADP
eurjchem-1541	23	11	α‐amylase	α‐amylase	NUM
eurjchem-1541	23	12	and	and	CCONJ
eurjchem-1541	23	13	α‐glucosidase	α‐glucosidase	PUNCT
eurjchem-1541	23	14	from	from	ADP
eurjchem-1541	23	15	medicinal	medicinal	ADJ
eurjchem-1541	23	16	plants	plant	NOUN
eurjchem-1541	23	17	to	to	PART
eurjchem-1541	23	18	treat	treat	VERB
eurjchem-1541	23	19	t2	t2	NOUN
eurjchem-1541	23	20	dm	dm	NUM
eurjchem-1541	24	1	[	[	X
eurjchem-1541	24	2	8‐11	8‐11	NUM
eurjchem-1541	24	3	]	]	X
eurjchem-1541	24	4	.	.	PUNCT
eurjchem-1541	25	1	for	for	ADP
eurjchem-1541	25	2	our	our	PRON
eurjchem-1541	25	3	part	part	NOUN
eurjchem-1541	25	4	,	,	PUNCT
eurjchem-1541	25	5	we	we	PRON
eurjchem-1541	25	6	study	study	VERB
eurjchem-1541	25	7	the	the	DET
eurjchem-1541	25	8	inhibitory	inhibitory	ADJ
eurjchem-1541	25	9	effect	effect	NOUN
eurjchem-1541	25	10	of	of	ADP
eurjchem-1541	25	11	α‐amylase	α‐amylase	NUM
eurjchem-1541	25	12	and	and	CCONJ
eurjchem-1541	25	13	α‐glucosidase	α‐glucosidase	PUNCT
eurjchem-1541	25	14	from	from	ADP
eurjchem-1541	25	15	chemical	chemical	ADJ
eurjchem-1541	25	16	synthesis	synthesis	NOUN
eurjchem-1541	25	17	products	product	NOUN
eurjchem-1541	25	18	derived	derive	VERB
eurjchem-1541	25	19	of	of	ADP
eurjchem-1541	25	20	pyrazolo[3,4‐d]pyrimidine	pyrazolo[3,4‐d]pyrimidine	NOUN
eurjchem-1541	25	21	.	.	PUNCT
eurjchem-1541	26	1	the	the	DET
eurjchem-1541	26	2	pyrazolo	pyrazolo	ADJ
eurjchem-1541	26	3	pyrimidine	pyrimidine	NOUN
eurjchem-1541	26	4	ring	ring	NOUN
eurjchem-1541	26	5	is	be	AUX
eurjchem-1541	26	6	very	very	ADV
eurjchem-1541	26	7	interesting	interesting	ADJ
eurjchem-1541	26	8	and	and	CCONJ
eurjchem-1541	26	9	versatile	versatile	ADJ
eurjchem-1541	26	10	scaffold	scaffold	NOUN
eurjchem-1541	26	11	for	for	ADP
eurjchem-1541	26	12	the	the	DET
eurjchem-1541	26	13	synthesis	synthesis	NOUN
eurjchem-1541	26	14	of	of	ADP
eurjchem-1541	26	15	potential	potential	ADJ
eurjchem-1541	26	16	drugs	drug	NOUN
eurjchem-1541	26	17	or	or	CCONJ
eurjchem-1541	26	18	molecular	molecular	ADJ
eurjchem-1541	26	19	tools	tool	NOUN
eurjchem-1541	26	20	(	(	PUNCT
eurjchem-1541	26	21	figure	figure	NOUN
eurjchem-1541	26	22	1	1	NUM
eurjchem-1541	26	23	)	)	PUNCT
eurjchem-1541	26	24	.	.	PUNCT
eurjchem-1541	27	1	the	the	DET
eurjchem-1541	27	2	derivatives	derivative	NOUN
eurjchem-1541	27	3	of	of	ADP
eurjchem-1541	27	4	pyrazolo[3,4‐d]pyrimidine	pyrazolo[3,4‐d]pyrimidine	NOUN
eurjchem-1541	27	5	constitute	constitute	VERB
eurjchem-1541	27	6	class	class	NOUN
eurjchem-1541	27	7	of	of	ADP
eurjchem-1541	27	8	heterocyclic	heterocyclic	ADJ
eurjchem-1541	27	9	compounds	compound	NOUN
eurjchem-1541	27	10	with	with	ADP
eurjchem-1541	27	11	interesting	interesting	ADJ
eurjchem-1541	27	12	pharmacological	pharmacological	ADJ
eurjchem-1541	27	13	properties	property	NOUN
eurjchem-1541	27	14	[	[	X
eurjchem-1541	27	15	12‐	12‐	NUM
eurjchem-1541	27	16	15	15	NUM
eurjchem-1541	27	17	]	]	PUNCT
eurjchem-1541	27	18	.	.	PUNCT
eurjchem-1541	28	1	among	among	ADP
eurjchem-1541	28	2	their	their	PRON
eurjchem-1541	28	3	many	many	ADJ
eurjchem-1541	28	4	applications	application	NOUN
eurjchem-1541	28	5	,	,	PUNCT
eurjchem-1541	28	6	they	they	PRON
eurjchem-1541	28	7	are	be	AUX
eurjchem-1541	28	8	widely	widely	ADV
eurjchem-1541	28	9	used	use	VERB
eurjchem-1541	28	10	for	for	ADP
eurjchem-1541	28	11	the	the	DET
eurjchem-1541	28	12	treatment	treatment	NOUN
eurjchem-1541	28	13	of	of	ADP
eurjchem-1541	28	14	gout	gout	NOUN
eurjchem-1541	29	1	[	[	X
eurjchem-1541	29	2	12	12	NUM
eurjchem-1541	29	3	]	]	PUNCT
eurjchem-1541	29	4	,	,	PUNCT
eurjchem-1541	29	5	hyperuricemia	hyperuricemia	NOUN
eurjchem-1541	30	1	[	[	X
eurjchem-1541	30	2	13	13	NUM
eurjchem-1541	30	3	]	]	PUNCT
eurjchem-1541	30	4	,	,	PUNCT
eurjchem-1541	30	5	treatment	treatment	NOUN
eurjchem-1541	30	6	and	and	CCONJ
eurjchem-1541	30	7	prevention	prevention	NOUN
eurjchem-1541	30	8	of	of	ADP
eurjchem-1541	30	9	uric	uric	ADJ
eurjchem-1541	30	10	acid	acid	NOUN
eurjchem-1541	31	1	[	[	X
eurjchem-1541	31	2	14	14	NUM
eurjchem-1541	31	3	]	]	PUNCT
eurjchem-1541	31	4	and	and	CCONJ
eurjchem-1541	31	5	also	also	ADV
eurjchem-1541	31	6	for	for	ADP
eurjchem-1541	31	7	the	the	DET
eurjchem-1541	31	8	treatment	treatment	NOUN
eurjchem-1541	31	9	of	of	ADP
eurjchem-1541	31	10	primary	primary	ADJ
eurjchem-1541	31	11	or	or	CCONJ
eurjchem-1541	31	12	secondary	secondary	ADJ
eurjchem-1541	31	13	symptomatic	symptomatic	ADJ
eurjchem-1541	31	14	hyperuricemia	hyperuricemia	NOUN
eurjchem-1541	32	1	[	[	X
eurjchem-1541	32	2	15	15	NUM
eurjchem-1541	32	3	]	]	PUNCT
eurjchem-1541	32	4	.	.	PUNCT
eurjchem-1541	33	1	in	in	ADP
eurjchem-1541	33	2	continuation	continuation	NOUN
eurjchem-1541	33	3	of	of	ADP
eurjchem-1541	33	4	our	our	PRON
eurjchem-1541	33	5	work	work	NOUN
eurjchem-1541	33	6	on	on	ADP
eurjchem-1541	33	7	the	the	DET
eurjchem-1541	33	8	synthesis	synthesis	NOUN
eurjchem-1541	33	9	of	of	ADP
eurjchem-1541	33	10	the	the	DET
eurjchem-1541	33	11	excess	excess	NOUN
eurjchem-1541	33	12	of	of	ADP
eurjchem-1541	33	13	allopurinol	allopurinol	NOUN
eurjchem-1541	33	14	[	[	X
eurjchem-1541	33	15	16‐23	16‐23	X
eurjchem-1541	33	16	]	]	PUNCT
eurjchem-1541	33	17	,	,	PUNCT
eurjchem-1541	33	18	we	we	PRON
eurjchem-1541	33	19	have	have	AUX
eurjchem-1541	33	20	envisioned	envision	VERB
eurjchem-1541	33	21	the	the	DET
eurjchem-1541	33	22	synthesis	synthesis	NOUN
eurjchem-1541	33	23	new	new	ADJ
eurjchem-1541	33	24	pyrazolo[3,4‐b]pyridine	pyrazolo[3,4‐b]pyridine	NOUN
eurjchem-1541	33	25	derivatives	derivative	NOUN
eurjchem-1541	33	26	by	by	ADP
eurjchem-1541	33	27	thionation	thionation	NOUN
eurjchem-1541	33	28	,	,	PUNCT
eurjchem-1541	33	29	alkylation	alkylation	NOUN
eurjchem-1541	33	30	and	and	CCONJ
eurjchem-1541	33	31	1,3‐dipolar	1,3‐dipolar	NUM
eurjchem-1541	33	32	cycloaddition	cycloaddition	NOUN
eurjchem-1541	33	33	reactions	reaction	NOUN
eurjchem-1541	33	34	in	in	ADP
eurjchem-1541	33	35	order	order	NOUN
eurjchem-1541	33	36	to	to	PART
eurjchem-1541	33	37	evaluate	evaluate	VERB
eurjchem-1541	33	38	their	their	PRON
eurjchem-1541	33	39	inhibitory	inhibitory	ADJ
eurjchem-1541	33	40	effect	effect	NOUN
eurjchem-1541	33	41	of	of	ADP
eurjchem-1541	33	42	α‐amylase	α‐amylase	NUM
eurjchem-1541	33	43	and	and	CCONJ
eurjchem-1541	33	44	α‐glucosidase	α‐glucosidase	SYM
eurjchem-1541	33	45	.	.	PROPN
eurjchem-1541	33	46	2	2	NUM
eurjchem-1541	33	47	.	.	X
eurjchem-1541	33	48	experimental	experimental	ADJ
eurjchem-1541	33	49	2.1	2.1	NUM
eurjchem-1541	33	50	.	.	PUNCT
eurjchem-1541	34	1	instrumentation	instrumentation	NOUN
eurjchem-1541	34	2	106	106	NUM
eurjchem-1541	34	3	el‐fal	el‐fal	NOUN
eurjchem-1541	34	4	et	et	PROPN
eurjchem-1541	34	5	al	al	PROPN
eurjchem-1541	34	6	.	.	PUNCT
eurjchem-1541	34	7	/	/	SYM
eurjchem-1541	34	8	european	european	PROPN
eurjchem-1541	34	9	journal	journal	PROPN
eurjchem-1541	34	10	of	of	ADP
eurjchem-1541	34	11	chemistry	chemistry	NOUN
eurjchem-1541	34	12	8	8	NUM
eurjchem-1541	34	13	(	(	PUNCT
eurjchem-1541	34	14	2	2	NUM
eurjchem-1541	34	15	)	)	PUNCT
eurjchem-1541	34	16	(	(	PUNCT
eurjchem-1541	34	17	2017	2017	NUM
eurjchem-1541	34	18	)	)	PUNCT
eurjchem-1541	34	19	105‐108	105‐108	NUM
eurjchem-1541	34	20	figure	figure	NOUN
eurjchem-1541	34	21	1	1	NUM
eurjchem-1541	34	22	.	.	PUNCT
eurjchem-1541	34	23	pyrazolopyrimidine	pyrazolopyrimidine	ADJ
eurjchem-1541	34	24	containing	contain	VERB
eurjchem-1541	34	25	drugs	drug	NOUN
eurjchem-1541	34	26	.	.	PUNCT
eurjchem-1541	35	1	the	the	DET
eurjchem-1541	35	2	melting	melting	NOUN
eurjchem-1541	35	3	points	point	NOUN
eurjchem-1541	35	4	were	be	AUX
eurjchem-1541	35	5	taken	take	VERB
eurjchem-1541	35	6	on	on	ADP
eurjchem-1541	35	7	an	an	DET
eurjchem-1541	35	8	electrothermal	electrothermal	ADJ
eurjchem-1541	35	9	capillary	capillary	ADJ
eurjchem-1541	35	10	melting	melting	NOUN
eurjchem-1541	35	11	point	point	NOUN
eurjchem-1541	35	12	apparatus	apparatus	NOUN
eurjchem-1541	35	13	.	.	PUNCT
eurjchem-1541	36	1	infrared	infrared	PROPN
eurjchem-1541	36	2	spectra	spectra	PROPN
eurjchem-1541	36	3	were	be	AUX
eurjchem-1541	36	4	recorded	record	VERB
eurjchem-1541	36	5	on	on	ADP
eurjchem-1541	36	6	a	a	DET
eurjchem-1541	36	7	perkin	perkin	PROPN
eurjchem-1541	36	8	elmer	elmer	PROPN
eurjchem-1541	36	9	577	577	NUM
eurjchem-1541	36	10	,	,	PUNCT
eurjchem-1541	36	11	using	use	VERB
eurjchem-1541	36	12	kbr	kbr	PROPN
eurjchem-1541	36	13	disks	disk	NOUN
eurjchem-1541	36	14	.	.	PUNCT
eurjchem-1541	37	1	1h	1h	NUM
eurjchem-1541	37	2	and	and	CCONJ
eurjchem-1541	37	3	13c	13c	NOUN
eurjchem-1541	37	4	nmr	nmr	NOUN
eurjchem-1541	37	5	spectra	spectra	NOUN
eurjchem-1541	37	6	were	be	AUX
eurjchem-1541	37	7	recorded	record	VERB
eurjchem-1541	37	8	on	on	ADP
eurjchem-1541	37	9	bruker	bruker	PROPN
eurjchem-1541	37	10	avance	avance	PROPN
eurjchem-1541	37	11	300	300	NUM
eurjchem-1541	37	12	nmr	nmr	NOUN
eurjchem-1541	37	13	spectrometer	spectrometer	NOUN
eurjchem-1541	37	14	in	in	ADP
eurjchem-1541	37	15	dmso‐d6	dmso‐d6	PROPN
eurjchem-1541	37	16	.	.	PUNCT
eurjchem-1541	38	1	spectra	spectra	PROPN
eurjchem-1541	38	2	were	be	AUX
eurjchem-1541	38	3	internally	internally	ADV
eurjchem-1541	38	4	referenced	reference	VERB
eurjchem-1541	38	5	to	to	ADP
eurjchem-1541	38	6	tms	tms	PROPN
eurjchem-1541	38	7	.	.	PUNCT
eurjchem-1541	39	1	peaks	peak	NOUN
eurjchem-1541	39	2	are	be	AUX
eurjchem-1541	39	3	reported	report	VERB
eurjchem-1541	39	4	in	in	ADP
eurjchem-1541	39	5	ppm	ppm	ADJ
eurjchem-1541	39	6	downfield	downfield	NOUN
eurjchem-1541	39	7	of	of	ADP
eurjchem-1541	39	8	tms	tms	PROPN
eurjchem-1541	39	9	.	.	PUNCT
eurjchem-1541	40	1	mass	mass	PROPN
eurjchem-1541	40	2	spectra	spectra	PROPN
eurjchem-1541	40	3	are	be	AUX
eurjchem-1541	40	4	recorded	record	VERB
eurjchem-1541	40	5	in	in	ADP
eurjchem-1541	40	6	a	a	DET
eurjchem-1541	40	7	synapt	synapt	NOUN
eurjchem-1541	40	8	g2	g2	PROPN
eurjchem-1541	40	9	hdms	hdms	PROPN
eurjchem-1541	40	10	,	,	PUNCT
eurjchem-1541	40	11	waters	water	NOUN
eurjchem-1541	40	12	,	,	PUNCT
eurjchem-1541	40	13	spectrometer	spectrometer	NOUN
eurjchem-1541	40	14	in	in	ADP
eurjchem-1541	40	15	electrospray	electrospray	NOUN
eurjchem-1541	40	16	ionization	ionization	NOUN
eurjchem-1541	40	17	(	(	PUNCT
eurjchem-1541	40	18	esi	esi	NOUN
eurjchem-1541	40	19	)	)	PUNCT
eurjchem-1541	40	20	.	.	PUNCT
eurjchem-1541	41	1	α‐amylase	α‐amylase	PUNCT
eurjchem-1541	42	1	and	and	CCONJ
eurjchem-1541	42	2	α‐glucosidase	α‐glucosidase	VERB
eurjchem-1541	42	3	inhibitory	inhibitory	ADJ
eurjchem-1541	42	4	activities	activity	NOUN
eurjchem-1541	42	5	were	be	AUX
eurjchem-1541	42	6	measured	measure	VERB
eurjchem-1541	42	7	using	use	VERB
eurjchem-1541	42	8	6705	6705	NUM
eurjchem-1541	42	9	uv	uv	NOUN
eurjchem-1541	42	10	/	/	SYM
eurjchem-1541	42	11	vis	vis	X
eurjchem-1541	42	12	spectrophotometer	spectrophotometer	X
eurjchem-1541	42	13	(	(	PUNCT
eurjchem-1541	42	14	jenway	jenway	PROPN
eurjchem-1541	42	15	)	)	PUNCT
eurjchem-1541	42	16	.	.	PUNCT
eurjchem-1541	43	1	2.2	2.2	NUM
eurjchem-1541	43	2	.	.	PUNCT
eurjchem-1541	43	3	thionation	thionation	NOUN
eurjchem-1541	43	4	of	of	ADP
eurjchem-1541	43	5	1h‐pyrazolo[3,4‐d]pyrimidin4(5h)‐one	1h‐pyrazolo[3,4‐d]pyrimidin4(5h)‐one	NUM
eurjchem-1541	43	6	the	the	DET
eurjchem-1541	43	7	thionation	thionation	NOUN
eurjchem-1541	43	8	reaction	reaction	NOUN
eurjchem-1541	43	9	was	be	AUX
eurjchem-1541	43	10	carried	carry	VERB
eurjchem-1541	43	11	out	out	ADP
eurjchem-1541	43	12	by	by	ADP
eurjchem-1541	43	13	the	the	DET
eurjchem-1541	43	14	action	action	NOUN
eurjchem-1541	43	15	of	of	ADP
eurjchem-1541	43	16	phosphorus	phosphorus	NOUN
eurjchem-1541	43	17	pentasulfide	pentasulfide	ADV
eurjchem-1541	43	18	on	on	ADP
eurjchem-1541	43	19	the	the	DET
eurjchem-1541	43	20	pyrazolo[3,4‐d]pyrimidine	pyrazolo[3,4‐d]pyrimidine	NOUN
eurjchem-1541	43	21	(	(	PUNCT
eurjchem-1541	43	22	a	a	NOUN
eurjchem-1541	43	23	)	)	PUNCT
eurjchem-1541	43	24	in	in	ADP
eurjchem-1541	43	25	pyridine	pyridine	NOUN
eurjchem-1541	43	26	[	[	X
eurjchem-1541	43	27	9	9	NUM
eurjchem-1541	43	28	]	]	PUNCT
eurjchem-1541	43	29	.	.	PUNCT
eurjchem-1541	44	1	the	the	DET
eurjchem-1541	44	2	reaction	reaction	NOUN
eurjchem-1541	44	3	leads	lead	VERB
eurjchem-1541	44	4	to	to	ADP
eurjchem-1541	44	5	pyrazolo[3,4‐	pyrazolo[3,4‐	NOUN
eurjchem-1541	44	6	d]pyrimidine‐4‐thione	d]pyrimidine‐4‐thione	X
eurjchem-1541	44	7	(	(	PUNCT
eurjchem-1541	44	8	b	b	NOUN
eurjchem-1541	44	9	)	)	PUNCT
eurjchem-1541	44	10	,	,	PUNCT
eurjchem-1541	44	11	with	with	ADP
eurjchem-1541	44	12	yield	yield	NOUN
eurjchem-1541	44	13	of	of	ADP
eurjchem-1541	44	14	90	90	NUM
eurjchem-1541	44	15	%	%	NOUN
eurjchem-1541	44	16	(	(	PUNCT
eurjchem-1541	44	17	scheme	scheme	NOUN
eurjchem-1541	44	18	1	1	NUM
eurjchem-1541	44	19	)	)	PUNCT
eurjchem-1541	44	20	.	.	PUNCT
eurjchem-1541	45	1	equimolar	equimolar	NOUN
eurjchem-1541	45	2	amounts	amount	NOUN
eurjchem-1541	45	3	of	of	ADP
eurjchem-1541	45	4	pyrazolo[3,4‐d]pyridine	pyrazolo[3,4‐d]pyridine	NOUN
eurjchem-1541	45	5	(	(	PUNCT
eurjchem-1541	45	6	3.67	3.67	NUM
eurjchem-1541	45	7	mmol	mmol	NOUN
eurjchem-1541	45	8	)	)	PUNCT
eurjchem-1541	45	9	and	and	CCONJ
eurjchem-1541	45	10	phosphorus	phosphorus	NOUN
eurjchem-1541	45	11	pentasulfide	pentasulfide	NOUN
eurjchem-1541	45	12	(	(	PUNCT
eurjchem-1541	45	13	3.67	3.67	NUM
eurjchem-1541	45	14	mmol	mmol	NOUN
eurjchem-1541	45	15	)	)	PUNCT
eurjchem-1541	45	16	in	in	ADP
eurjchem-1541	45	17	pyridine	pyridine	NOUN
eurjchem-1541	45	18	was	be	AUX
eurjchem-1541	45	19	heated	heat	VERB
eurjchem-1541	45	20	to	to	PART
eurjchem-1541	45	21	reflux	reflux	VERB
eurjchem-1541	45	22	for	for	ADP
eurjchem-1541	45	23	4	4	NUM
eurjchem-1541	45	24	hours	hour	NOUN
eurjchem-1541	45	25	.	.	PUNCT
eurjchem-1541	46	1	then	then	ADV
eurjchem-1541	46	2	the	the	DET
eurjchem-1541	46	3	solvent	solvent	NOUN
eurjchem-1541	46	4	is	be	AUX
eurjchem-1541	46	5	evapo‐	evapo‐	VERB
eurjchem-1541	46	6	rated	rate	VERB
eurjchem-1541	46	7	under	under	ADP
eurjchem-1541	46	8	reduced	reduced	ADJ
eurjchem-1541	46	9	pressure	pressure	NOUN
eurjchem-1541	46	10	,	,	PUNCT
eurjchem-1541	46	11	the	the	DET
eurjchem-1541	46	12	precipitate	precipitate	NOUN
eurjchem-1541	46	13	formed	form	VERB
eurjchem-1541	46	14	is	be	AUX
eurjchem-1541	46	15	washed	wash	VERB
eurjchem-1541	46	16	with	with	ADP
eurjchem-1541	46	17	hot	hot	ADJ
eurjchem-1541	46	18	water	water	NOUN
eurjchem-1541	46	19	to	to	PART
eurjchem-1541	46	20	remove	remove	VERB
eurjchem-1541	46	21	residual	residual	ADJ
eurjchem-1541	46	22	dimerized	dimerize	VERB
eurjchem-1541	46	23	p2s5	p2s5	PROPN
eurjchem-1541	46	24	.	.	PROPN
eurjchem-1541	46	25	1h,4h,5h‐pyrazolo[3,4‐d]pyrimidine‐4‐thione	1h,4h,5h‐pyrazolo[3,4‐d]pyrimidine‐4‐thione	NUM
eurjchem-1541	46	26	(	(	PUNCT
eurjchem-1541	46	27	b	b	NOUN
eurjchem-1541	46	28	):	):	PUNCT
eurjchem-1541	46	29	color	color	NOUN
eurjchem-1541	46	30	:	:	PUNCT
eurjchem-1541	46	31	yellow	yellow	ADJ
eurjchem-1541	46	32	.	.	PUNCT
eurjchem-1541	47	1	yield	yield	NOUN
eurjchem-1541	47	2	:	:	PUNCT
eurjchem-1541	47	3	90	90	NUM
eurjchem-1541	47	4	%	%	NOUN
eurjchem-1541	47	5	.	.	PUNCT
eurjchem-1541	48	1	m.p	m.p	PROPN
eurjchem-1541	48	2	.	.	PROPN
eurjchem-1541	48	3	:	:	PUNCT
eurjchem-1541	49	1	189‐199	189‐199	PROPN
eurjchem-1541	49	2	°	°	SYM
eurjchem-1541	49	3	c	c	X
eurjchem-1541	49	4	.	.	PUNCT
eurjchem-1541	50	1	ft‐ir	ft‐ir	NOUN
eurjchem-1541	50	2	(	(	PUNCT
eurjchem-1541	50	3	kbr	kbr	PROPN
eurjchem-1541	50	4	,	,	PUNCT
eurjchem-1541	50	5	ν	ν	PROPN
eurjchem-1541	50	6	,	,	PUNCT
eurjchem-1541	50	7	cm‐1	cm‐1	PROPN
eurjchem-1541	50	8	):	):	PUNCT
eurjchem-1541	50	9	1110	1110	NUM
eurjchem-1541	50	10	(c	(c	PROPN
eurjchem-1541	50	11	=	=	SYM
eurjchem-1541	50	12	s	s	NOUN
eurjchem-1541	50	13	)	)	PUNCT
eurjchem-1541	50	14	.	.	PUNCT
eurjchem-1541	51	1	1h	1h	NUM
eurjchem-1541	51	2	nmr	nmr	NOUN
eurjchem-1541	51	3	(	(	PUNCT
eurjchem-1541	51	4	300	300	NUM
eurjchem-1541	51	5	mhz	mhz	NOUN
eurjchem-1541	51	6	,	,	PUNCT
eurjchem-1541	51	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1541	51	8	,	,	PUNCT
eurjchem-1541	51	9	δ	δ	PROPN
eurjchem-1541	51	10	,	,	PUNCT
eurjchem-1541	51	11	ppm	ppm	NUM
eurjchem-1541	51	12	):	):	PUNCT
eurjchem-1541	51	13	13.74	13.74	NUM
eurjchem-1541	51	14	(	(	PUNCT
eurjchem-1541	51	15	s	s	PROPN
eurjchem-1541	51	16	,	,	PUNCT
eurjchem-1541	51	17	1h	1h	NUM
eurjchem-1541	51	18	,	,	PUNCT
eurjchem-1541	51	19	nh	nh	PROPN
eurjchem-1541	51	20	)	)	PUNCT
eurjchem-1541	51	21	,	,	PUNCT
eurjchem-1541	51	22	13.13	13.13	NUM
eurjchem-1541	51	23	(	(	PUNCT
eurjchem-1541	51	24	s	s	PROPN
eurjchem-1541	51	25	,	,	PUNCT
eurjchem-1541	51	26	1h	1h	NUM
eurjchem-1541	51	27	,	,	PUNCT
eurjchem-1541	51	28	nh	nh	PROPN
eurjchem-1541	51	29	)	)	PUNCT
eurjchem-1541	51	30	,	,	PUNCT
eurjchem-1541	51	31	8.16	8.16	NUM
eurjchem-1541	51	32	(	(	PUNCT
eurjchem-1541	51	33	s	s	PROPN
eurjchem-1541	51	34	,	,	PUNCT
eurjchem-1541	51	35	1h	1h	NUM
eurjchem-1541	51	36	,	,	PUNCT
eurjchem-1541	51	37	=	=	NOUN
eurjchem-1541	51	38	ch	ch	NOUN
eurjchem-1541	51	39	)	)	PUNCT
eurjchem-1541	51	40	,	,	PUNCT
eurjchem-1541	51	41	8.01	8.01	NUM
eurjchem-1541	51	42	(	(	PUNCT
eurjchem-1541	51	43	s	s	PROPN
eurjchem-1541	51	44	,	,	PUNCT
eurjchem-1541	51	45	1h	1h	NUM
eurjchem-1541	51	46	,	,	PUNCT
eurjchem-1541	51	47	=	=	NOUN
eurjchem-1541	51	48	ch	ch	NOUN
eurjchem-1541	51	49	)	)	PUNCT
eurjchem-1541	51	50	.	.	PUNCT
eurjchem-1541	52	1	13c	13c	NOUN
eurjchem-1541	52	2	nmr	nmr	NOUN
eurjchem-1541	52	3	(	(	PUNCT
eurjchem-1541	52	4	75	75	NUM
eurjchem-1541	52	5	mhz	mhz	NOUN
eurjchem-1541	52	6	,	,	PUNCT
eurjchem-1541	52	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1541	52	8	,	,	PUNCT
eurjchem-1541	52	9	δ	δ	PROPN
eurjchem-1541	52	10	,	,	PUNCT
eurjchem-1541	52	11	ppm	ppm	NUM
eurjchem-1541	52	12	):	):	PUNCT
eurjchem-1541	52	13	133.36	133.36	NUM
eurjchem-1541	52	14	(=	(=	NOUN
eurjchem-1541	52	15	ch	ch	NOUN
eurjchem-1541	52	16	)	)	PUNCT
eurjchem-1541	52	17	,	,	PUNCT
eurjchem-1541	52	18	134.66	134.66	NUM
eurjchem-1541	52	19	(=	(=	NOUN
eurjchem-1541	52	20	ch	ch	NOUN
eurjchem-1541	52	21	)	)	PUNCT
eurjchem-1541	52	22	,	,	PUNCT
eurjchem-1541	52	23	105.17	105.17	NUM
eurjchem-1541	52	24	,	,	PUNCT
eurjchem-1541	52	25	146.84	146.84	NUM
eurjchem-1541	52	26	,	,	PUNCT
eurjchem-1541	52	27	157.19	157.19	NUM
eurjchem-1541	52	28	(	(	PUNCT
eurjchem-1541	52	29	cq	cq	NOUN
eurjchem-1541	52	30	)	)	PUNCT
eurjchem-1541	52	31	.	.	PUNCT
eurjchem-1541	53	1	ms	ms	PROPN
eurjchem-1541	53	2	(	(	PUNCT
eurjchem-1541	53	3	esi	esi	PROPN
eurjchem-1541	53	4	,	,	PUNCT
eurjchem-1541	53	5	m	m	PROPN
eurjchem-1541	53	6	/	/	SYM
eurjchem-1541	53	7	z	z	NOUN
eurjchem-1541	53	8	):	):	PUNCT
eurjchem-1541	53	9	153.0	153.0	NUM
eurjchem-1541	53	10	.	.	PUNCT
eurjchem-1541	54	1	scheme	scheme	NOUN
eurjchem-1541	54	2	1	1	NUM
eurjchem-1541	54	3	2.3	2.3	NUM
eurjchem-1541	54	4	.	.	PUNCT
eurjchem-1541	55	1	general	general	ADJ
eurjchem-1541	55	2	procedure	procedure	NOUN
eurjchem-1541	55	3	for	for	ADP
eurjchem-1541	55	4	the	the	DET
eurjchem-1541	55	5	synthesis	synthesis	NOUN
eurjchem-1541	55	6	of(alkysulfanyl)‐	of(alkysulfanyl)‐	NOUN
eurjchem-1541	55	7	1h‐pyrazolo[3,4‐d]pyrimidine	1h‐pyrazolo[3,4‐d]pyrimidine	NUM
eurjchem-1541	55	8	1h,4h,5h‐pyrazolo[3,4‐d]pyrimidine‐4‐thione	1h,4h,5h‐pyrazolo[3,4‐d]pyrimidine‐4‐thione	NUM
eurjchem-1541	55	9	(	(	PUNCT
eurjchem-1541	55	10	3.29	3.29	NUM
eurjchem-1541	55	11	mmol	mmol	NOUN
eurjchem-1541	55	12	)	)	PUNCT
eurjchem-1541	55	13	,	,	PUNCT
eurjchem-1541	55	14	alkyl	alkyl	ADJ
eurjchem-1541	55	15	bromide	bromide	NOUN
eurjchem-1541	55	16	(	(	PUNCT
eurjchem-1541	55	17	5.70	5.70	NUM
eurjchem-1541	55	18	mmol	mmol	NOUN
eurjchem-1541	55	19	)	)	PUNCT
eurjchem-1541	55	20	and	and	CCONJ
eurjchem-1541	55	21	potassium	potassium	NOUN
eurjchem-1541	55	22	carbonate	carbonate	NOUN
eurjchem-1541	55	23	(	(	PUNCT
eurjchem-1541	55	24	4.8	4.8	NUM
eurjchem-1541	55	25	mmol	mmol	NOUN
eurjchem-1541	55	26	)	)	PUNCT
eurjchem-1541	55	27	with	with	ADP
eurjchem-1541	55	28	a	a	DET
eurjchem-1541	55	29	catalytic	catalytic	ADJ
eurjchem-1541	55	30	amount	amount	NOUN
eurjchem-1541	55	31	of	of	ADP
eurjchem-1541	55	32	tetra‐n‐butylammonium	tetra‐n‐butylammonium	NOUN
eurjchem-1541	55	33	bromide	bromide	NOUN
eurjchem-1541	55	34	were	be	AUX
eurjchem-1541	55	35	stirred	stir	VERB
eurjchem-1541	55	36	in	in	ADP
eurjchem-1541	55	37	dmf	dmf	PROPN
eurjchem-1541	55	38	(	(	PUNCT
eurjchem-1541	55	39	15	15	NUM
eurjchem-1541	55	40	ml	ml	NOUN
eurjchem-1541	55	41	)	)	PUNCT
eurjchem-1541	55	42	for	for	ADP
eurjchem-1541	55	43	48‐72	48‐72	NUM
eurjchem-1541	55	44	h.	h.	NOUN
eurjchem-1541	56	1	the	the	DET
eurjchem-1541	56	2	solid	solid	ADJ
eurjchem-1541	56	3	obtained	obtain	VERB
eurjchem-1541	56	4	was	be	AUX
eurjchem-1541	56	5	removed	remove	VERB
eurjchem-1541	56	6	by	by	ADP
eurjchem-1541	56	7	filtration	filtration	NOUN
eurjchem-1541	56	8	and	and	CCONJ
eurjchem-1541	56	9	the	the	DET
eurjchem-1541	56	10	solvent	solvent	NOUN
eurjchem-1541	56	11	evaporated	evaporate	VERB
eurjchem-1541	56	12	under	under	ADP
eurjchem-1541	56	13	vacuum	vacuum	NOUN
eurjchem-1541	56	14	.	.	PUNCT
eurjchem-1541	57	1	the	the	DET
eurjchem-1541	57	2	solid	solid	ADJ
eurjchem-1541	57	3	product	product	NOUN
eurjchem-1541	57	4	was	be	AUX
eurjchem-1541	57	5	purified	purify	VERB
eurjchem-1541	57	6	by	by	ADP
eurjchem-1541	57	7	recrystallization	recrystallization	NOUN
eurjchem-1541	57	8	from	from	ADP
eurjchem-1541	57	9	ethanol	ethanol	NOUN
eurjchem-1541	57	10	(	(	PUNCT
eurjchem-1541	57	11	scheme	scheme	NOUN
eurjchem-1541	57	12	2	2	NUM
eurjchem-1541	57	13	)	)	PUNCT
eurjchem-1541	57	14	.	.	PUNCT
eurjchem-1541	58	1	4‐(allylsulfanyl)‐1h‐pyrazolo[3,4‐d]pyrimidine	4‐(allylsulfanyl)‐1h‐pyrazolo[3,4‐d]pyrimidine	PROPN
eurjchem-1541	58	2	(	(	PUNCT
eurjchem-1541	58	3	c	c	NOUN
eurjchem-1541	58	4	):	):	PUNCT
eurjchem-1541	58	5	color	color	NOUN
eurjchem-1541	58	6	:	:	PUNCT
eurjchem-1541	58	7	white	white	ADJ
eurjchem-1541	58	8	.	.	PUNCT
eurjchem-1541	59	1	yield	yield	NOUN
eurjchem-1541	59	2	:	:	PUNCT
eurjchem-1541	59	3	60	60	NUM
eurjchem-1541	59	4	%	%	NOUN
eurjchem-1541	59	5	.	.	PUNCT
eurjchem-1541	60	1	m.p	m.p	PROPN
eurjchem-1541	60	2	.	.	PROPN
eurjchem-1541	60	3	:	:	PUNCT
eurjchem-1541	61	1	140‐150	140‐150	NUM
eurjchem-1541	61	2	°	°	PROPN
eurjchem-1541	61	3	c	c	X
eurjchem-1541	61	4	.	.	PUNCT
eurjchem-1541	62	1	ft‐ir	ft‐ir	NOUN
eurjchem-1541	62	2	(	(	PUNCT
eurjchem-1541	62	3	kbr	kbr	PROPN
eurjchem-1541	62	4	,	,	PUNCT
eurjchem-1541	62	5	ν	ν	PROPN
eurjchem-1541	62	6	,	,	PUNCT
eurjchem-1541	62	7	cm‐1	cm‐1	PROPN
eurjchem-1541	62	8	):	):	PUNCT
eurjchem-1541	62	9	1100	1100	NUM
eurjchem-1541	62	10	(c‐s	(c‐s	NOUN
eurjchem-1541	62	11	)	)	PUNCT
eurjchem-1541	62	12	.	.	PUNCT
eurjchem-1541	63	1	1h	1h	NUM
eurjchem-1541	63	2	nmr	nmr	NOUN
eurjchem-1541	63	3	(	(	PUNCT
eurjchem-1541	63	4	300	300	NUM
eurjchem-1541	63	5	mhz	mhz	NOUN
eurjchem-1541	63	6	,	,	PUNCT
eurjchem-1541	63	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1541	63	8	,	,	PUNCT
eurjchem-1541	63	9	δ	δ	PROPN
eurjchem-1541	63	10	,	,	PUNCT
eurjchem-1541	63	11	ppm	ppm	NOUN
eurjchem-1541	63	12	):	):	PUNCT
eurjchem-1541	63	13	14.09	14.09	NUM
eurjchem-1541	63	14	(	(	PUNCT
eurjchem-1541	63	15	s	s	PROPN
eurjchem-1541	63	16	,	,	PUNCT
eurjchem-1541	63	17	1h	1h	NUM
eurjchem-1541	63	18	,	,	PUNCT
eurjchem-1541	63	19	nh	nh	PROPN
eurjchem-1541	63	20	)	)	PUNCT
eurjchem-1541	63	21	,	,	PUNCT
eurjchem-1541	63	22	8.72	8.72	NUM
eurjchem-1541	63	23	(	(	PUNCT
eurjchem-1541	63	24	s	s	PROPN
eurjchem-1541	63	25	,	,	PUNCT
eurjchem-1541	63	26	1h	1h	NUM
eurjchem-1541	63	27	,	,	PUNCT
eurjchem-1541	63	28	=	=	NOUN
eurjchem-1541	63	29	ch	ch	NOUN
eurjchem-1541	63	30	)	)	PUNCT
eurjchem-1541	63	31	,	,	PUNCT
eurjchem-1541	63	32	8.27	8.27	NUM
eurjchem-1541	63	33	(	(	PUNCT
eurjchem-1541	63	34	s	s	PROPN
eurjchem-1541	63	35	,	,	PUNCT
eurjchem-1541	63	36	1h,=ch	1h,=ch	NUM
eurjchem-1541	63	37	)	)	PUNCT
eurjchem-1541	63	38	,	,	PUNCT
eurjchem-1541	63	39	4.02‐4.09	4.02‐4.09	PROPN
eurjchem-1541	63	40	(	(	PUNCT
eurjchem-1541	63	41	d	d	NOUN
eurjchem-1541	63	42	,	,	PUNCT
eurjchem-1541	63	43	2h	2h	NUM
eurjchem-1541	63	44	,	,	PUNCT
eurjchem-1541	63	45	sch2	sch2	PROPN
eurjchem-1541	63	46	,	,	PUNCT
eurjchem-1541	63	47	j	j	PROPN
eurjchem-1541	64	1	=	=	PROPN
eurjchem-1541	64	2	2.48	2.48	NUM
eurjchem-1541	64	3	hz	hz	NOUN
eurjchem-1541	64	4	)	)	PUNCT
eurjchem-1541	64	5	,	,	PUNCT
eurjchem-1541	64	6	5.16‐5.39	5.16‐5.39	NUM
eurjchem-1541	64	7	(	(	PUNCT
eurjchem-1541	64	8	d	d	NOUN
eurjchem-1541	64	9	,	,	PUNCT
eurjchem-1541	64	10	2h	2h	NUM
eurjchem-1541	64	11	,	,	PUNCT
eurjchem-1541	64	12	=	=	NOUN
eurjchem-1541	64	13	ch2	ch2	X
eurjchem-1541	64	14	,	,	PUNCT
eurjchem-1541	64	15	j	j	PROPN
eurjchem-1541	65	1	=	=	PROPN
eurjchem-1541	65	2	5.16	5.16	NUM
eurjchem-1541	65	3	hz	hz	NOUN
eurjchem-1541	65	4	)	)	PUNCT
eurjchem-1541	65	5	,	,	PUNCT
eurjchem-1541	65	6	5.94‐6.02	5.94‐6.02	NUM
eurjchem-1541	65	7	(	(	PUNCT
eurjchem-1541	65	8	m	m	PROPN
eurjchem-1541	65	9	,	,	PUNCT
eurjchem-1541	65	10	1h	1h	NUM
eurjchem-1541	65	11	,	,	PUNCT
eurjchem-1541	65	12	=	=	NOUN
eurjchem-1541	65	13	ch	ch	NOUN
eurjchem-1541	65	14	,	,	PUNCT
eurjchem-1541	65	15	j	j	X
eurjchem-1541	66	1	=	=	PROPN
eurjchem-1541	66	2	5.98	5.98	NUM
eurjchem-1541	66	3	hz	hz	NOUN
eurjchem-1541	66	4	)	)	PUNCT
eurjchem-1541	66	5	.	.	PUNCT
eurjchem-1541	67	1	13c	13c	NOUN
eurjchem-1541	67	2	nmr	nmr	NOUN
eurjchem-1541	67	3	(	(	PUNCT
eurjchem-1541	67	4	75	75	NUM
eurjchem-1541	67	5	mhz	mhz	NOUN
eurjchem-1541	67	6	,	,	PUNCT
eurjchem-1541	67	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1541	67	8	,	,	PUNCT
eurjchem-1541	67	9	δ	δ	PROPN
eurjchem-1541	67	10	,	,	PUNCT
eurjchem-1541	67	11	ppm	ppm	NUM
eurjchem-1541	67	12	):	):	PUNCT
eurjchem-1541	67	13	15.11	15.11	NUM
eurjchem-1541	67	14	(	(	PUNCT
eurjchem-1541	67	15	sch2	sch2	PROPN
eurjchem-1541	67	16	)	)	PUNCT
eurjchem-1541	67	17	,	,	PUNCT
eurjchem-1541	67	18	132.62	132.62	NUM
eurjchem-1541	67	19	,	,	PUNCT
eurjchem-1541	67	20	152.16	152.16	NUM
eurjchem-1541	67	21	(=	(=	NOUN
eurjchem-1541	67	22	ch	ch	NOUN
eurjchem-1541	67	23	)	)	PUNCT
eurjchem-1541	67	24	,	,	PUNCT
eurjchem-1541	67	25	111.50	111.50	NUM
eurjchem-1541	67	26	,	,	PUNCT
eurjchem-1541	67	27	154.49	154.49	NUM
eurjchem-1541	67	28	,	,	PUNCT
eurjchem-1541	67	29	164.37	164.37	NUM
eurjchem-1541	67	30	(	(	PUNCT
eurjchem-1541	67	31	cq	cq	NOUN
eurjchem-1541	67	32	)	)	PUNCT
eurjchem-1541	67	33	.	.	PUNCT
eurjchem-1541	68	1	ms	ms	PROPN
eurjchem-1541	68	2	(	(	PUNCT
eurjchem-1541	68	3	esi	esi	PROPN
eurjchem-1541	68	4	,	,	PUNCT
eurjchem-1541	68	5	m	m	PROPN
eurjchem-1541	68	6	/	/	SYM
eurjchem-1541	68	7	z	z	NOUN
eurjchem-1541	68	8	):	):	PUNCT
eurjchem-1541	68	9	193.1	193.1	NUM
eurjchem-1541	68	10	4‐(prop‐2‐ynylsulfanyl)‐1h‐pyrazolo[3,4‐d]pyrimidine	4‐(prop‐2‐ynylsulfanyl)‐1h‐pyrazolo[3,4‐d]pyrimidine	NUM
eurjchem-1541	68	11	(	(	PUNCT
eurjchem-1541	68	12	d	d	NOUN
eurjchem-1541	68	13	):	):	PUNCT
eurjchem-1541	68	14	color	color	NOUN
eurjchem-1541	68	15	:	:	PUNCT
eurjchem-1541	68	16	white	white	ADJ
eurjchem-1541	68	17	.	.	PUNCT
eurjchem-1541	68	18	yield	yield	NOUN
eurjchem-1541	68	19	:	:	PUNCT
eurjchem-1541	68	20	70	70	NUM
eurjchem-1541	68	21	%	%	NOUN
eurjchem-1541	68	22	.	.	PUNCT
eurjchem-1541	69	1	m.p	m.p	PROPN
eurjchem-1541	69	2	.	.	PROPN
eurjchem-1541	69	3	:	:	PUNCT
eurjchem-1541	70	1	130‐140	130‐140	NUM
eurjchem-1541	70	2	°	°	NUM
eurjchem-1541	70	3	c	c	X
eurjchem-1541	70	4	.	.	PUNCT
eurjchem-1541	71	1	ft‐ir	ft‐ir	NOUN
eurjchem-1541	71	2	(	(	PUNCT
eurjchem-1541	71	3	kbr	kbr	PROPN
eurjchem-1541	71	4	,	,	PUNCT
eurjchem-1541	71	5	ν	ν	PROPN
eurjchem-1541	71	6	,	,	PUNCT
eurjchem-1541	71	7	cm‐	cm‐	NOUN
eurjchem-1541	71	8	1	1	NUM
eurjchem-1541	71	9	):	):	PUNCT
eurjchem-1541	71	10	1100	1100	NUM
eurjchem-1541	71	11	(c‐s	(c‐s	NOUN
eurjchem-1541	71	12	)	)	PUNCT
eurjchem-1541	71	13	.	.	PUNCT
eurjchem-1541	72	1	1h	1h	NUM
eurjchem-1541	72	2	nmr	nmr	NOUN
eurjchem-1541	72	3	(	(	PUNCT
eurjchem-1541	72	4	300	300	NUM
eurjchem-1541	72	5	mhz	mhz	NOUN
eurjchem-1541	72	6	,	,	PUNCT
eurjchem-1541	72	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1541	72	8	,	,	PUNCT
eurjchem-1541	72	9	δ	δ	PROPN
eurjchem-1541	72	10	,	,	PUNCT
eurjchem-1541	72	11	ppm	ppm	NUM
eurjchem-1541	72	12	):	):	PUNCT
eurjchem-1541	72	13	13.98	13.98	NUM
eurjchem-1541	72	14	(	(	PUNCT
eurjchem-1541	72	15	s	s	PROPN
eurjchem-1541	72	16	,	,	PUNCT
eurjchem-1541	72	17	1h	1h	NUM
eurjchem-1541	72	18	,	,	PUNCT
eurjchem-1541	72	19	nh	nh	PROPN
eurjchem-1541	72	20	)	)	PUNCT
eurjchem-1541	72	21	,	,	PUNCT
eurjchem-1541	72	22	8.62	8.62	NUM
eurjchem-1541	72	23	(	(	PUNCT
eurjchem-1541	72	24	s	s	PROPN
eurjchem-1541	72	25	,	,	PUNCT
eurjchem-1541	72	26	1h	1h	NUM
eurjchem-1541	72	27	,	,	PUNCT
eurjchem-1541	72	28	=	=	NOUN
eurjchem-1541	72	29	ch	ch	NOUN
eurjchem-1541	72	30	)	)	PUNCT
eurjchem-1541	72	31	,	,	PUNCT
eurjchem-1541	72	32	8.23	8.23	NUM
eurjchem-1541	72	33	(	(	PUNCT
eurjchem-1541	72	34	s	s	PROPN
eurjchem-1541	72	35	,	,	PUNCT
eurjchem-1541	72	36	1h	1h	NUM
eurjchem-1541	72	37	,	,	PUNCT
eurjchem-1541	72	38	=	=	NOUN
eurjchem-1541	72	39	ch	ch	NOUN
eurjchem-1541	72	40	)	)	PUNCT
eurjchem-1541	72	41	,	,	PUNCT
eurjchem-1541	72	42	1.98	1.98	NUM
eurjchem-1541	72	43	(	(	PUNCT
eurjchem-1541	72	44	s	s	PROPN
eurjchem-1541	72	45	,	,	PUNCT
eurjchem-1541	72	46	1h	1h	NUM
eurjchem-1541	72	47	,	,	PUNCT
eurjchem-1541	72	48	c≡h	c≡h	PROPN
eurjchem-1541	72	49	)	)	PUNCT
eurjchem-1541	72	50	,	,	PUNCT
eurjchem-1541	72	51	4.03	4.03	NUM
eurjchem-1541	72	52	(	(	PUNCT
eurjchem-1541	72	53	s	s	PROPN
eurjchem-1541	72	54	,	,	PUNCT
eurjchem-1541	72	55	2h	2h	NUM
eurjchem-1541	72	56	,	,	PUNCT
eurjchem-1541	72	57	sch2	sch2	PROPN
eurjchem-1541	72	58	)	)	PUNCT
eurjchem-1541	72	59	.	.	PUNCT
eurjchem-1541	73	1	13c	13c	NOUN
eurjchem-1541	73	2	nmr	nmr	NOUN
eurjchem-1541	73	3	(	(	PUNCT
eurjchem-1541	73	4	75	75	NUM
eurjchem-1541	73	5	mhz	mhz	NOUN
eurjchem-1541	73	6	,	,	PUNCT
eurjchem-1541	73	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1541	73	8	,	,	PUNCT
eurjchem-1541	73	9	δ	δ	PROPN
eurjchem-1541	73	10	,	,	PUNCT
eurjchem-1541	73	11	ppm	ppm	NOUN
eurjchem-1541	73	12	):	):	PUNCT
eurjchem-1541	73	13	21.09	21.09	NUM
eurjchem-1541	73	14	(	(	PUNCT
eurjchem-1541	73	15	sch2	sch2	PROPN
eurjchem-1541	73	16	)	)	PUNCT
eurjchem-1541	73	17	,	,	PUNCT
eurjchem-1541	73	18	73.01	73.01	NUM
eurjchem-1541	73	19	(	(	PUNCT
eurjchem-1541	73	20	hc≡	hc≡	PROPN
eurjchem-1541	73	21	)	)	PUNCT
eurjchem-1541	73	22	,	,	PUNCT
eurjchem-1541	73	23	133.03	133.03	NUM
eurjchem-1541	73	24	,	,	PUNCT
eurjchem-1541	73	25	155.07	155.07	NUM
eurjchem-1541	73	26	(=	(=	NOUN
eurjchem-1541	73	27	ch	ch	NOUN
eurjchem-1541	73	28	)	)	PUNCT
eurjchem-1541	73	29	,	,	PUNCT
eurjchem-1541	73	30	78.01	78.01	NUM
eurjchem-1541	73	31	,	,	PUNCT
eurjchem-1541	73	32	112.415	112.415	NUM
eurjchem-1541	73	33	,	,	PUNCT
eurjchem-1541	73	34	155.07	155.07	NUM
eurjchem-1541	73	35	,	,	PUNCT
eurjchem-1541	73	36	162.39	162.39	NUM
eurjchem-1541	73	37	(	(	PUNCT
eurjchem-1541	73	38	cq	cq	NOUN
eurjchem-1541	73	39	)	)	PUNCT
eurjchem-1541	73	40	.	.	PUNCT
eurjchem-1541	74	1	ms	ms	PROPN
eurjchem-1541	74	2	(	(	PUNCT
eurjchem-1541	74	3	esi	esi	PROPN
eurjchem-1541	74	4	,	,	PUNCT
eurjchem-1541	74	5	m	m	PROPN
eurjchem-1541	74	6	/	/	SYM
eurjchem-1541	74	7	z	z	NOUN
eurjchem-1541	74	8	):	):	PUNCT
eurjchem-1541	74	9	191.0	191.0	NUM
eurjchem-1541	74	10	.	.	PUNCT
eurjchem-1541	75	1	4‐benzylsulfanyl‐1h‐pyrazolo[3,4‐d]‐pyrimidine	4‐benzylsulfanyl‐1h‐pyrazolo[3,4‐d]‐pyrimidine	NUM
eurjchem-1541	75	2	(	(	PUNCT
eurjchem-1541	75	3	e	e	NOUN
eurjchem-1541	75	4	):	):	PUNCT
eurjchem-1541	75	5	color	color	NOUN
eurjchem-1541	75	6	:	:	PUNCT
eurjchem-1541	75	7	yellow	yellow	ADJ
eurjchem-1541	75	8	.	.	PUNCT
eurjchem-1541	76	1	yield	yield	NOUN
eurjchem-1541	76	2	:	:	PUNCT
eurjchem-1541	76	3	70	70	NUM
eurjchem-1541	76	4	%	%	NOUN
eurjchem-1541	76	5	.	.	PUNCT
eurjchem-1541	77	1	m.p	m.p	PROPN
eurjchem-1541	77	2	.	.	PROPN
eurjchem-1541	77	3	:	:	PUNCT
eurjchem-1541	78	1	150‐166	150‐166	NUM
eurjchem-1541	78	2	°	°	SYM
eurjchem-1541	78	3	c	c	NOUN
eurjchem-1541	78	4	.	.	PUNCT
eurjchem-1541	79	1	ft‐ir	ft‐ir	NOUN
eurjchem-1541	79	2	(	(	PUNCT
eurjchem-1541	79	3	kbr	kbr	PROPN
eurjchem-1541	79	4	,	,	PUNCT
eurjchem-1541	79	5	ν	ν	PROPN
eurjchem-1541	79	6	,	,	PUNCT
eurjchem-1541	79	7	cm‐1	cm‐1	PROPN
eurjchem-1541	79	8	):	):	PUNCT
eurjchem-1541	79	9	1100	1100	NUM
eurjchem-1541	79	10	(c	(c	PROPN
eurjchem-1541	79	11	=	=	SYM
eurjchem-1541	79	12	s	s	NOUN
eurjchem-1541	79	13	)	)	PUNCT
eurjchem-1541	79	14	.	.	PUNCT
eurjchem-1541	80	1	1h	1h	NUM
eurjchem-1541	80	2	nmr	nmr	NOUN
eurjchem-1541	80	3	(	(	PUNCT
eurjchem-1541	80	4	300	300	NUM
eurjchem-1541	80	5	mhz	mhz	NOUN
eurjchem-1541	80	6	,	,	PUNCT
eurjchem-1541	80	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1541	80	8	,	,	PUNCT
eurjchem-1541	80	9	δ	δ	PROPN
eurjchem-1541	80	10	,	,	PUNCT
eurjchem-1541	80	11	ppm	ppm	NOUN
eurjchem-1541	80	12	):	):	PUNCT
eurjchem-1541	80	13	14.09	14.09	NUM
eurjchem-1541	80	14	(	(	PUNCT
eurjchem-1541	80	15	s	s	PROPN
eurjchem-1541	80	16	,	,	PUNCT
eurjchem-1541	80	17	1h	1h	NUM
eurjchem-1541	80	18	,	,	PUNCT
eurjchem-1541	80	19	nh	nh	PROPN
eurjchem-1541	80	20	)	)	PUNCT
eurjchem-1541	80	21	,	,	PUNCT
eurjchem-1541	80	22	8.76	8.76	NUM
eurjchem-1541	80	23	(	(	PUNCT
eurjchem-1541	80	24	s	s	PROPN
eurjchem-1541	80	25	,	,	PUNCT
eurjchem-1541	80	26	1h	1h	NUM
eurjchem-1541	80	27	,	,	PUNCT
eurjchem-1541	80	28	=	=	NOUN
eurjchem-1541	80	29	ch	ch	NOUN
eurjchem-1541	80	30	)	)	PUNCT
eurjchem-1541	80	31	,	,	PUNCT
eurjchem-1541	80	32	8.25	8.25	NUM
eurjchem-1541	80	33	(	(	PUNCT
eurjchem-1541	80	34	s	s	PROPN
eurjchem-1541	80	35	,	,	PUNCT
eurjchem-1541	80	36	1h	1h	NUM
eurjchem-1541	80	37	,	,	PUNCT
eurjchem-1541	80	38	=	=	NOUN
eurjchem-1541	80	39	ch	ch	NOUN
eurjchem-1541	80	40	)	)	PUNCT
eurjchem-1541	80	41	,	,	PUNCT
eurjchem-1541	80	42	7.20‐7.45	7.20‐7.45	NUM
eurjchem-1541	80	43	(	(	PUNCT
eurjchem-1541	80	44	m	m	PROPN
eurjchem-1541	80	45	,	,	PUNCT
eurjchem-1541	80	46	5h	5h	NUM
eurjchem-1541	80	47	,	,	PUNCT
eurjchem-1541	80	48	ar‐	ar‐	PROPN
eurjchem-1541	80	49	h	h	NOUN
eurjchem-1541	80	50	)	)	PUNCT
eurjchem-1541	80	51	,	,	PUNCT
eurjchem-1541	80	52	4.65	4.65	NUM
eurjchem-1541	80	53	(	(	PUNCT
eurjchem-1541	80	54	s	s	PROPN
eurjchem-1541	80	55	,	,	PUNCT
eurjchem-1541	80	56	2h	2h	NUM
eurjchem-1541	80	57	,	,	PUNCT
eurjchem-1541	80	58	sch2	sch2	PROPN
eurjchem-1541	80	59	)	)	PUNCT
eurjchem-1541	80	60	.	.	PUNCT
eurjchem-1541	81	1	13c	13c	NOUN
eurjchem-1541	81	2	nmr	nmr	NOUN
eurjchem-1541	81	3	(	(	PUNCT
eurjchem-1541	81	4	75	75	NUM
eurjchem-1541	81	5	mhz	mhz	NOUN
eurjchem-1541	81	6	,	,	PUNCT
eurjchem-1541	81	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1541	81	8	,	,	PUNCT
eurjchem-1541	81	9	δ	δ	PROPN
eurjchem-1541	81	10	,	,	PUNCT
eurjchem-1541	81	11	ppm	ppm	NUM
eurjchem-1541	81	12	):	):	PUNCT
eurjchem-1541	81	13	32.44	32.44	NUM
eurjchem-1541	81	14	(	(	PUNCT
eurjchem-1541	81	15	sch2	sch2	PROPN
eurjchem-1541	81	16	)	)	PUNCT
eurjchem-1541	81	17	,	,	PUNCT
eurjchem-1541	81	18	132.60	132.60	NUM
eurjchem-1541	81	19	,	,	PUNCT
eurjchem-1541	81	20	152.77	152.77	NUM
eurjchem-1541	81	21	(=	(=	NOUN
eurjchem-1541	81	22	ch	ch	NOUN
eurjchem-1541	81	23	)	)	PUNCT
eurjchem-1541	81	24	,	,	PUNCT
eurjchem-1541	81	25	111.15	111.15	NUM
eurjchem-1541	81	26	,	,	PUNCT
eurjchem-1541	81	27	127.78	127.78	NUM
eurjchem-1541	81	28	,	,	PUNCT
eurjchem-1541	81	29	129.00	129.00	NUM
eurjchem-1541	81	30	,	,	PUNCT
eurjchem-1541	81	31	129.50	129.50	NUM
eurjchem-1541	81	32	,	,	PUNCT
eurjchem-1541	81	33	173.73	173.73	NUM
eurjchem-1541	81	34	,	,	PUNCT
eurjchem-1541	81	35	152.77	152.77	NUM
eurjchem-1541	81	36	,	,	PUNCT
eurjchem-1541	81	37	154.45	154.45	NUM
eurjchem-1541	81	38	,	,	PUNCT
eurjchem-1541	81	39	163.94	163.94	NUM
eurjchem-1541	81	40	(	(	PUNCT
eurjchem-1541	81	41	cq	cq	NOUN
eurjchem-1541	81	42	)	)	PUNCT
eurjchem-1541	81	43	.	.	PUNCT
eurjchem-1541	82	1	ms	ms	PROPN
eurjchem-1541	82	2	(	(	PUNCT
eurjchem-1541	82	3	esi	esi	PROPN
eurjchem-1541	82	4	,	,	PUNCT
eurjchem-1541	82	5	m	m	PROPN
eurjchem-1541	82	6	/	/	SYM
eurjchem-1541	82	7	z	z	NOUN
eurjchem-1541	82	8	):	):	PUNCT
eurjchem-1541	82	9	242.2	242.2	NUM
eurjchem-1541	82	10	.	.	PUNCT
eurjchem-1541	82	11	scheme	scheme	VERB
eurjchem-1541	82	12	2	2	NUM
eurjchem-1541	82	13	2.4	2.4	NUM
eurjchem-1541	82	14	.	.	PUNCT
eurjchem-1541	82	15	general	general	ADJ
eurjchem-1541	82	16	procedure	procedure	NOUN
eurjchem-1541	82	17	for	for	ADP
eurjchem-1541	82	18	the	the	DET
eurjchem-1541	82	19	synthesis	synthesis	NOUN
eurjchem-1541	82	20	of	of	ADP
eurjchem-1541	82	21	cycloadduct	cycloadduct	NOUN
eurjchem-1541	82	22	f	f	PROPN
eurjchem-1541	82	23	and	and	CCONJ
eurjchem-1541	82	24	g	g	NOUN
eurjchem-1541	82	25	to	to	ADP
eurjchem-1541	82	26	a	a	DET
eurjchem-1541	82	27	solution	solution	NOUN
eurjchem-1541	82	28	of	of	ADP
eurjchem-1541	82	29	4‐(prop‐2‐ynylsulfanyl)‐1h‐pyrazolo[3,4‐	4‐(prop‐2‐ynylsulfanyl)‐1h‐pyrazolo[3,4‐	NUM
eurjchem-1541	82	30	d]pyrimidine	d]pyrimidine	X
eurjchem-1541	82	31	(	(	PUNCT
eurjchem-1541	82	32	4.4	4.4	NUM
eurjchem-1541	82	33	mmol	mmol	NOUN
eurjchem-1541	82	34	)	)	PUNCT
eurjchem-1541	82	35	and	and	CCONJ
eurjchem-1541	82	36	2‐chlorobenzaldoxime	2‐chlorobenzaldoxime	NUM
eurjchem-1541	82	37	/benzaldoxime	/benzaldoxime	PUNCT
eurjchem-1541	82	38	(	(	PUNCT
eurjchem-1541	82	39	6.4	6.4	NUM
eurjchem-1541	82	40	mmol	mmol	NOUN
eurjchem-1541	82	41	)	)	PUNCT
eurjchem-1541	82	42	in	in	ADP
eurjchem-1541	82	43	60	60	NUM
eurjchem-1541	82	44	ml	ml	NOUN
eurjchem-1541	82	45	of	of	ADP
eurjchem-1541	82	46	chloroform	chloroform	NOUN
eurjchem-1541	82	47	was	be	AUX
eurjchem-1541	82	48	added	add	VERB
eurjchem-1541	82	49	30	30	NUM
eurjchem-1541	82	50	ml	ml	NOUN
eurjchem-1541	82	51	of	of	ADP
eurjchem-1541	82	52	liquid	liquid	ADJ
eurjchem-1541	82	53	bleach	bleach	NOUN
eurjchem-1541	82	54	with	with	ADP
eurjchem-1541	82	55	vigorous	vigorous	ADJ
eurjchem-1541	82	56	stirring	stirring	NOUN
eurjchem-1541	82	57	for	for	ADP
eurjchem-1541	82	58	2	2	NUM
eurjchem-1541	82	59	hours	hour	NOUN
eurjchem-1541	82	60	.	.	PUNCT
eurjchem-1541	83	1	the	the	DET
eurjchem-1541	83	2	organic	organic	ADJ
eurjchem-1541	83	3	phase	phase	NOUN
eurjchem-1541	83	4	obtained	obtain	VERB
eurjchem-1541	83	5	was	be	AUX
eurjchem-1541	83	6	dried	dry	VERB
eurjchem-1541	83	7	over	over	ADP
eurjchem-1541	83	8	sodium	sodium	NOUN
eurjchem-1541	83	9	sulphate	sulphate	NOUN
eurjchem-1541	83	10	,	,	PUNCT
eurjchem-1541	83	11	concentrated	concentrate	VERB
eurjchem-1541	83	12	under	under	ADP
eurjchem-1541	83	13	reduced	reduced	ADJ
eurjchem-1541	83	14	pressure	pressure	NOUN
eurjchem-1541	83	15	.	.	PUNCT
eurjchem-1541	84	1	the	the	DET
eurjchem-1541	84	2	residue	residue	NOUN
eurjchem-1541	84	3	obtained	obtain	VERB
eurjchem-1541	84	4	was	be	AUX
eurjchem-1541	84	5	chromatographed	chromatographe	VERB
eurjchem-1541	84	6	on	on	ADP
eurjchem-1541	84	7	silica	silica	NOUN
eurjchem-1541	84	8	gel	gel	NOUN
eurjchem-1541	84	9	(	(	PUNCT
eurjchem-1541	84	10	hexane	hexane	NOUN
eurjchem-1541	84	11	:	:	PUNCT
eurjchem-1541	84	12	ethyl	ethyl	PROPN
eurjchem-1541	84	13	acetate	acetate	NOUN
eurjchem-1541	84	14	,	,	PUNCT
eurjchem-1541	84	15	80:20	80:20	NUM
eurjchem-1541	84	16	,	,	PUNCT
eurjchem-1541	84	17	v	v	NOUN
eurjchem-1541	84	18	:	:	SYM
eurjchem-1541	84	19	v	v	NOUN
eurjchem-1541	84	20	)	)	PUNCT
eurjchem-1541	84	21	(	(	PUNCT
eurjchem-1541	84	22	scheme	scheme	NOUN
eurjchem-1541	84	23	3	3	NUM
eurjchem-1541	84	24	)	)	PUNCT
eurjchem-1541	84	25	.	.	PUNCT
eurjchem-1541	85	1	4‐((3‐phenylisoxazol‐5‐yl)methylsulfanyl)‐1h‐pyrazolo[3,4‐	4‐((3‐phenylisoxazol‐5‐yl)methylsulfanyl)‐1h‐pyrazolo[3,4‐	NUM
eurjchem-1541	85	2	d]pyrimidine	d]pyrimidine	INTJ
eurjchem-1541	85	3	(	(	PUNCT
eurjchem-1541	85	4	f	f	X
eurjchem-1541	85	5	):	):	PUNCT
eurjchem-1541	85	6	color	color	NOUN
eurjchem-1541	85	7	:	:	PUNCT
eurjchem-1541	85	8	white	white	ADJ
eurjchem-1541	85	9	.	.	PUNCT
eurjchem-1541	86	1	yield	yield	NOUN
eurjchem-1541	86	2	:	:	PUNCT
eurjchem-1541	86	3	40	40	NUM
eurjchem-1541	86	4	%	%	NOUN
eurjchem-1541	86	5	.	.	PUNCT
eurjchem-1541	87	1	m.p	m.p	PROPN
eurjchem-1541	87	2	.	.	PROPN
eurjchem-1541	87	3	:	:	PUNCT
eurjchem-1541	88	1	120‐124	120‐124	NUM
eurjchem-1541	88	2	°	°	ADP
eurjchem-1541	88	3	c	c	X
eurjchem-1541	88	4	.	.	PUNCT
eurjchem-1541	89	1	ft‐ir	ft‐ir	NOUN
eurjchem-1541	89	2	(	(	PUNCT
eurjchem-1541	89	3	kbr	kbr	PROPN
eurjchem-1541	89	4	,	,	PUNCT
eurjchem-1541	89	5	ν	ν	PROPN
eurjchem-1541	89	6	,	,	PUNCT
eurjchem-1541	89	7	cm‐1	cm‐1	PROPN
eurjchem-1541	89	8	):	):	PUNCT
eurjchem-1541	89	9	1100	1100	NUM
eurjchem-1541	89	10	(c	(c	PROPN
eurjchem-1541	89	11	=	=	SYM
eurjchem-1541	89	12	s	s	NOUN
eurjchem-1541	89	13	)	)	PUNCT
eurjchem-1541	89	14	.	.	PUNCT
eurjchem-1541	90	1	1h	1h	NUM
eurjchem-1541	90	2	nmr	nmr	NOUN
eurjchem-1541	90	3	(	(	PUNCT
eurjchem-1541	90	4	300	300	NUM
eurjchem-1541	90	5	mhz	mhz	NOUN
eurjchem-1541	90	6	,	,	PUNCT
eurjchem-1541	90	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1541	90	8	,	,	PUNCT
eurjchem-1541	90	9	δ	δ	PROPN
eurjchem-1541	90	10	,	,	PUNCT
eurjchem-1541	90	11	ppm	ppm	NUM
eurjchem-1541	90	12	):	):	PUNCT
eurjchem-1541	90	13	14.10	14.10	NUM
eurjchem-1541	90	14	(	(	PUNCT
eurjchem-1541	90	15	s	s	PROPN
eurjchem-1541	90	16	,	,	PUNCT
eurjchem-1541	90	17	1h	1h	NUM
eurjchem-1541	90	18	,	,	PUNCT
eurjchem-1541	90	19	nh	nh	PROPN
eurjchem-1541	90	20	)	)	PUNCT
eurjchem-1541	90	21	,	,	PUNCT
eurjchem-1541	90	22	8.09	8.09	NUM
eurjchem-1541	90	23	(	(	PUNCT
eurjchem-1541	90	24	s	s	PROPN
eurjchem-1541	90	25	,	,	PUNCT
eurjchem-1541	90	26	1h	1h	NUM
eurjchem-1541	90	27	,	,	PUNCT
eurjchem-1541	90	28	ch	ch	NOUN
eurjchem-1541	90	29	)	)	PUNCT
eurjchem-1541	90	30	,	,	PUNCT
eurjchem-1541	90	31	7.99	7.99	NUM
eurjchem-1541	90	32	(	(	PUNCT
eurjchem-1541	90	33	s	s	PROPN
eurjchem-1541	90	34	,	,	PUNCT
eurjchem-1541	90	35	1h	1h	NUM
eurjchem-1541	90	36	,	,	PUNCT
eurjchem-1541	90	37	ch	ch	NOUN
eurjchem-1541	90	38	)	)	PUNCT
eurjchem-1541	90	39	,	,	PUNCT
eurjchem-1541	90	40	6.83‐7.97	6.83‐7.97	NOUN
eurjchem-1541	90	41	(	(	PUNCT
eurjchem-1541	90	42	m	m	PROPN
eurjchem-1541	90	43	,	,	PUNCT
eurjchem-1541	90	44	5h	5h	NUM
eurjchem-1541	90	45	,	,	PUNCT
eurjchem-1541	90	46	j	j	PROPN
eurjchem-1541	90	47	=	=	SYM
eurjchem-1541	90	48	7.7	7.7	NUM
eurjchem-1541	90	49	hz	hz	NOUN
eurjchem-1541	90	50	,	,	PUNCT
eurjchem-1541	90	51	ar‐h	ar‐h	PROPN
eurjchem-1541	90	52	)	)	PUNCT
eurjchem-1541	90	53	,	,	PUNCT
eurjchem-1541	90	54	5.53	5.53	NUM
eurjchem-1541	90	55	(	(	PUNCT
eurjchem-1541	90	56	s	s	PROPN
eurjchem-1541	90	57	,	,	PUNCT
eurjchem-1541	90	58	1h	1h	NUM
eurjchem-1541	90	59	,	,	PUNCT
eurjchem-1541	90	60	ch	ch	NOUN
eurjchem-1541	90	61	)	)	PUNCT
eurjchem-1541	90	62	,	,	PUNCT
eurjchem-1541	90	63	4.52	4.52	NUM
eurjchem-1541	90	64	(	(	PUNCT
eurjchem-1541	90	65	d	d	NOUN
eurjchem-1541	90	66	,	,	PUNCT
eurjchem-1541	90	67	2h	2h	NUM
eurjchem-1541	90	68	,	,	PUNCT
eurjchem-1541	90	69	j	j	PROPN
eurjchem-1541	90	70	=	=	SYM
eurjchem-1541	90	71	7.2	7.2	NUM
eurjchem-1541	90	72	hz	hz	NOUN
eurjchem-1541	90	73	,	,	PUNCT
eurjchem-1541	90	74	sch2	sch2	PROPN
eurjchem-1541	90	75	)	)	PUNCT
eurjchem-1541	90	76	.	.	PUNCT
eurjchem-1541	91	1	el‐fal	el‐fal	PROPN
eurjchem-1541	91	2	et	et	PROPN
eurjchem-1541	91	3	al	al	PROPN
eurjchem-1541	91	4	.	.	PUNCT
eurjchem-1541	91	5	/	/	SYM
eurjchem-1541	91	6	european	european	PROPN
eurjchem-1541	91	7	journal	journal	PROPN
eurjchem-1541	91	8	of	of	ADP
eurjchem-1541	91	9	chemistry	chemistry	NOUN
eurjchem-1541	91	10	8	8	NUM
eurjchem-1541	91	11	(	(	PUNCT
eurjchem-1541	91	12	2	2	NUM
eurjchem-1541	91	13	)	)	PUNCT
eurjchem-1541	91	14	(	(	PUNCT
eurjchem-1541	91	15	2017	2017	NUM
eurjchem-1541	91	16	)	)	PUNCT
eurjchem-1541	91	17	105‐108	105‐108	PROPN
eurjchem-1541	91	18	107	107	NUM
eurjchem-1541	91	19	scheme	scheme	NOUN
eurjchem-1541	91	20	3	3	NUM
eurjchem-1541	91	21	13c	13c	NOUN
eurjchem-1541	91	22	nmr	nmr	NOUN
eurjchem-1541	91	23	(	(	PUNCT
eurjchem-1541	91	24	75	75	NUM
eurjchem-1541	91	25	mhz	mhz	NOUN
eurjchem-1541	91	26	,	,	PUNCT
eurjchem-1541	91	27	dmso‐d6	dmso‐d6	PROPN
eurjchem-1541	91	28	,	,	PUNCT
eurjchem-1541	91	29	δ	δ	PROPN
eurjchem-1541	91	30	,	,	PUNCT
eurjchem-1541	91	31	ppm	ppm	NUM
eurjchem-1541	91	32	):	):	PUNCT
eurjchem-1541	91	33	33.61	33.61	NUM
eurjchem-1541	91	34	(	(	PUNCT
eurjchem-1541	91	35	ch2	ch2	PROPN
eurjchem-1541	91	36	)	)	PUNCT
eurjchem-1541	91	37	,	,	PUNCT
eurjchem-1541	91	38	100.80	100.80	NUM
eurjchem-1541	91	39	(	(	PUNCT
eurjchem-1541	91	40	chisoxazolique	chisoxazolique	NOUN
eurjchem-1541	91	41	)	)	PUNCT
eurjchem-1541	91	42	,	,	PUNCT
eurjchem-1541	91	43	99.70	99.70	NUM
eurjchem-1541	91	44	,	,	PUNCT
eurjchem-1541	91	45	100.79	100.79	NUM
eurjchem-1541	91	46	,	,	PUNCT
eurjchem-1541	91	47	117.03	117.03	NUM
eurjchem-1541	91	48	,	,	PUNCT
eurjchem-1541	91	49	126.38	126.38	NUM
eurjchem-1541	91	50	,	,	PUNCT
eurjchem-1541	91	51	133.23	133.23	NUM
eurjchem-1541	91	52	(	(	PUNCT
eurjchem-1541	91	53	cq	cq	NOUN
eurjchem-1541	91	54	)	)	PUNCT
eurjchem-1541	91	55	,	,	PUNCT
eurjchem-1541	91	56	129.26	129.26	NUM
eurjchem-1541	91	57	,	,	PUNCT
eurjchem-1541	91	58	142.20	142.20	NUM
eurjchem-1541	91	59	(	(	PUNCT
eurjchem-1541	91	60	char	char	PROPN
eurjchem-1541	91	61	)	)	PUNCT
eurjchem-1541	91	62	,	,	PUNCT
eurjchem-1541	91	63	143.87	143.87	NUM
eurjchem-1541	91	64	(	(	PUNCT
eurjchem-1541	91	65	ch	ch	NOUN
eurjchem-1541	91	66	)	)	PUNCT
eurjchem-1541	91	67	,	,	PUNCT
eurjchem-1541	91	68	148.01	148.01	NUM
eurjchem-1541	91	69	(	(	PUNCT
eurjchem-1541	91	70	ch	ch	NOUN
eurjchem-1541	91	71	)	)	PUNCT
eurjchem-1541	91	72	.	.	PUNCT
eurjchem-1541	92	1	ms	ms	PROPN
eurjchem-1541	92	2	(	(	PUNCT
eurjchem-1541	92	3	esi	esi	PROPN
eurjchem-1541	92	4	,	,	PUNCT
eurjchem-1541	92	5	m	m	PROPN
eurjchem-1541	92	6	/	/	SYM
eurjchem-1541	92	7	z	z	NOUN
eurjchem-1541	92	8	):	):	PUNCT
eurjchem-1541	92	9	309.0	309.0	NUM
eurjchem-1541	92	10	.	.	PUNCT
eurjchem-1541	93	1	4‐((3‐(2‐chlorophenyl)isoxazol‐5‐yl)methylsulfanyl)‐1h‐	4‐((3‐(2‐chlorophenyl)isoxazol‐5‐yl)methylsulfanyl)‐1h‐	NUM
eurjchem-1541	93	2	pyrazolo[3,4‐d]pyrimidine	pyrazolo[3,4‐d]pyrimidine	NOUN
eurjchem-1541	93	3	(	(	PUNCT
eurjchem-1541	93	4	g	g	NOUN
eurjchem-1541	93	5	):	):	PUNCT
eurjchem-1541	93	6	color	color	NOUN
eurjchem-1541	93	7	:	:	PUNCT
eurjchem-1541	93	8	yellow	yellow	ADJ
eurjchem-1541	93	9	.	.	PUNCT
eurjchem-1541	94	1	yield	yield	NOUN
eurjchem-1541	94	2	:	:	PUNCT
eurjchem-1541	94	3	40	40	NUM
eurjchem-1541	94	4	%	%	NOUN
eurjchem-1541	94	5	.	.	PUNCT
eurjchem-1541	95	1	m.p	m.p	PROPN
eurjchem-1541	95	2	:	:	PUNCT
eurjchem-1541	95	3	110‐120	110‐120	PROPN
eurjchem-1541	95	4	°	°	PROPN
eurjchem-1541	95	5	c	c	PROPN
eurjchem-1541	95	6	.	.	PUNCT
eurjchem-1541	96	1	ft‐ir	ft‐ir	NOUN
eurjchem-1541	96	2	(	(	PUNCT
eurjchem-1541	96	3	kbr	kbr	PROPN
eurjchem-1541	96	4	,	,	PUNCT
eurjchem-1541	96	5	ν	ν	PROPN
eurjchem-1541	96	6	,	,	PUNCT
eurjchem-1541	96	7	cm‐1	cm‐1	PROPN
eurjchem-1541	96	8	):	):	PUNCT
eurjchem-1541	96	9	1100	1100	NUM
eurjchem-1541	96	10	(c	(c	PROPN
eurjchem-1541	96	11	=	=	SYM
eurjchem-1541	96	12	s	s	NOUN
eurjchem-1541	96	13	)	)	PUNCT
eurjchem-1541	96	14	.	.	PUNCT
eurjchem-1541	97	1	1h	1h	NUM
eurjchem-1541	97	2	nmr	nmr	NOUN
eurjchem-1541	97	3	(	(	PUNCT
eurjchem-1541	97	4	300	300	NUM
eurjchem-1541	97	5	mhz	mhz	NOUN
eurjchem-1541	97	6	,	,	PUNCT
eurjchem-1541	97	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1541	97	8	,	,	PUNCT
eurjchem-1541	97	9	δ	δ	PROPN
eurjchem-1541	97	10	,	,	PUNCT
eurjchem-1541	97	11	ppm	ppm	NUM
eurjchem-1541	97	12	):	):	PUNCT
eurjchem-1541	97	13	14.06	14.06	NUM
eurjchem-1541	97	14	(	(	PUNCT
eurjchem-1541	97	15	s	s	PROPN
eurjchem-1541	97	16	,	,	PUNCT
eurjchem-1541	97	17	1h	1h	NUM
eurjchem-1541	97	18	,	,	PUNCT
eurjchem-1541	97	19	nh	nh	PROPN
eurjchem-1541	97	20	)	)	PUNCT
eurjchem-1541	97	21	,	,	PUNCT
eurjchem-1541	97	22	8.72	8.72	NUM
eurjchem-1541	97	23	(	(	PUNCT
eurjchem-1541	97	24	s	s	PROPN
eurjchem-1541	97	25	,	,	PUNCT
eurjchem-1541	97	26	1h	1h	NUM
eurjchem-1541	97	27	,	,	PUNCT
eurjchem-1541	97	28	ch	ch	NOUN
eurjchem-1541	97	29	)	)	PUNCT
eurjchem-1541	97	30	,	,	PUNCT
eurjchem-1541	97	31	8.71	8.71	NUM
eurjchem-1541	97	32	(	(	PUNCT
eurjchem-1541	97	33	s	s	PROPN
eurjchem-1541	97	34	,	,	PUNCT
eurjchem-1541	97	35	1h	1h	NUM
eurjchem-1541	97	36	,	,	PUNCT
eurjchem-1541	97	37	ch	ch	NOUN
eurjchem-1541	97	38	)	)	PUNCT
eurjchem-1541	97	39	,	,	PUNCT
eurjchem-1541	97	40	5.49‐5.99	5.49‐5.99	NUM
eurjchem-1541	97	41	(	(	PUNCT
eurjchem-1541	97	42	m	m	PROPN
eurjchem-1541	97	43	,	,	PUNCT
eurjchem-1541	97	44	j	j	PROPN
eurjchem-1541	97	45	=	=	SYM
eurjchem-1541	97	46	7.7	7.7	NUM
eurjchem-1541	97	47	hz	hz	NOUN
eurjchem-1541	97	48	,	,	PUNCT
eurjchem-1541	97	49	4h	4h	NOUN
eurjchem-1541	97	50	,	,	PUNCT
eurjchem-1541	97	51	ar‐h	ar‐h	PROPN
eurjchem-1541	97	52	)	)	PUNCT
eurjchem-1541	97	53	,	,	PUNCT
eurjchem-1541	97	54	5.30	5.30	NUM
eurjchem-1541	97	55	(	(	PUNCT
eurjchem-1541	97	56	s	s	PROPN
eurjchem-1541	97	57	,	,	PUNCT
eurjchem-1541	97	58	1h	1h	NUM
eurjchem-1541	97	59	,	,	PUNCT
eurjchem-1541	97	60	ch	ch	NOUN
eurjchem-1541	97	61	)	)	PUNCT
eurjchem-1541	97	62	,	,	PUNCT
eurjchem-1541	97	63	4.03	4.03	NUM
eurjchem-1541	97	64	(	(	PUNCT
eurjchem-1541	97	65	d	d	NOUN
eurjchem-1541	97	66	,	,	PUNCT
eurjchem-1541	97	67	2h	2h	NUM
eurjchem-1541	97	68	,	,	PUNCT
eurjchem-1541	97	69	j	j	PROPN
eurjchem-1541	97	70	=	=	SYM
eurjchem-1541	97	71	7.2	7.2	NUM
eurjchem-1541	97	72	hz	hz	NOUN
eurjchem-1541	97	73	,	,	PUNCT
eurjchem-1541	97	74	sch2	sch2	PROPN
eurjchem-1541	97	75	)	)	PUNCT
eurjchem-1541	97	76	.	.	PUNCT
eurjchem-1541	98	1	13c	13c	NOUN
eurjchem-1541	98	2	nmr	nmr	NOUN
eurjchem-1541	98	3	(	(	PUNCT
eurjchem-1541	98	4	75	75	NUM
eurjchem-1541	98	5	mhz	mhz	NOUN
eurjchem-1541	98	6	,	,	PUNCT
eurjchem-1541	98	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1541	98	8	,	,	PUNCT
eurjchem-1541	98	9	δ	δ	PROPN
eurjchem-1541	98	10	,	,	PUNCT
eurjchem-1541	98	11	ppm	ppm	NUM
eurjchem-1541	98	12	):	):	PUNCT
eurjchem-1541	98	13	31.22	31.22	NUM
eurjchem-1541	98	14	(	(	PUNCT
eurjchem-1541	98	15	ch2	ch2	PROPN
eurjchem-1541	98	16	)	)	PUNCT
eurjchem-1541	98	17	,	,	PUNCT
eurjchem-1541	98	18	111.39	111.39	NUM
eurjchem-1541	98	19	(	(	PUNCT
eurjchem-1541	98	20	ch	ch	NOUN
eurjchem-1541	98	21	)	)	PUNCT
eurjchem-1541	98	22	,	,	PUNCT
eurjchem-1541	98	23	111.70	111.70	NUM
eurjchem-1541	98	24	,	,	PUNCT
eurjchem-1541	98	25	118.86	118.86	NUM
eurjchem-1541	98	26	,	,	PUNCT
eurjchem-1541	98	27	119.03	119.03	NUM
eurjchem-1541	98	28	,	,	PUNCT
eurjchem-1541	98	29	125.37	125.37	NUM
eurjchem-1541	98	30	,	,	PUNCT
eurjchem-1541	98	31	126.23	126.23	NUM
eurjchem-1541	98	32	(	(	PUNCT
eurjchem-1541	98	33	cq	cq	NOUN
eurjchem-1541	98	34	)	)	PUNCT
eurjchem-1541	98	35	,	,	PUNCT
eurjchem-1541	98	36	132.07	132.07	NUM
eurjchem-1541	98	37	,	,	PUNCT
eurjchem-1541	98	38	133.67	133.67	NUM
eurjchem-1541	98	39	(	(	PUNCT
eurjchem-1541	98	40	ar‐c	ar‐c	PROPN
eurjchem-1541	98	41	)	)	PUNCT
eurjchem-1541	98	42	,	,	PUNCT
eurjchem-1541	98	43	154.29	154.29	NUM
eurjchem-1541	98	44	(	(	PUNCT
eurjchem-1541	98	45	ch	ch	NOUN
eurjchem-1541	98	46	)	)	PUNCT
eurjchem-1541	98	47	,	,	PUNCT
eurjchem-1541	98	48	157.44	157.44	NUM
eurjchem-1541	98	49	(	(	PUNCT
eurjchem-1541	98	50	ch	ch	NOUN
eurjchem-1541	98	51	)	)	PUNCT
eurjchem-1541	98	52	.	.	PUNCT
eurjchem-1541	99	1	ms	ms	PROPN
eurjchem-1541	99	2	(	(	PUNCT
eurjchem-1541	99	3	esi	esi	PROPN
eurjchem-1541	99	4	,	,	PUNCT
eurjchem-1541	99	5	m	m	PROPN
eurjchem-1541	99	6	/	/	SYM
eurjchem-1541	99	7	z	z	NOUN
eurjchem-1541	99	8	):	):	PUNCT
eurjchem-1541	99	9	343.3	343.3	NUM
eurjchem-1541	99	10	.	.	X
eurjchem-1541	99	11	2.5	2.5	NUM
eurjchem-1541	99	12	.	.	PUNCT
eurjchem-1541	99	13	in‐vitro	in‐vitro	VERB
eurjchem-1541	99	14	α‐amylase	α‐amylase	NUM
eurjchem-1541	99	15	and	and	CCONJ
eurjchem-1541	99	16	α‐glucosidase	α‐glucosidase	PUNCT
eurjchem-1541	99	17	inhibitory	inhibitory	ADJ
eurjchem-1541	99	18	activity	activity	NOUN
eurjchem-1541	99	19	2.5.1	2.5.1	NUM
eurjchem-1541	99	20	.	.	PUNCT
eurjchem-1541	100	1	α‐amylase	α‐amylase	AUX
eurjchem-1541	100	2	inhibitory	inhibitory	ADJ
eurjchem-1541	100	3	assay	assay	NOUN
eurjchem-1541	100	4	α‐amylase	α‐amylase	VERB
eurjchem-1541	100	5	inhibitory	inhibitory	ADJ
eurjchem-1541	100	6	activity	activity	NOUN
eurjchem-1541	100	7	of	of	ADP
eurjchem-1541	100	8	the	the	DET
eurjchem-1541	100	9	synthetic	synthetic	ADJ
eurjchem-1541	100	10	compounds	compound	NOUN
eurjchem-1541	100	11	was	be	AUX
eurjchem-1541	100	12	determined	determine	VERB
eurjchem-1541	100	13	as	as	ADP
eurjchem-1541	100	14	previously	previously	ADV
eurjchem-1541	100	15	described	describe	VERB
eurjchem-1541	100	16	method	method	NOUN
eurjchem-1541	100	17	[	[	X
eurjchem-1541	100	18	24	24	NUM
eurjchem-1541	100	19	]	]	PUNCT
eurjchem-1541	100	20	.	.	PUNCT
eurjchem-1541	101	1	a	a	DET
eurjchem-1541	101	2	total	total	NOUN
eurjchem-1541	101	3	of	of	ADP
eurjchem-1541	101	4	250	250	NUM
eurjchem-1541	101	5	μl	μl	ADP
eurjchem-1541	101	6	of	of	ADP
eurjchem-1541	101	7	samples	sample	NOUN
eurjchem-1541	101	8	and	and	CCONJ
eurjchem-1541	101	9	250	250	NUM
eurjchem-1541	101	10	μl	μl	ADP
eurjchem-1541	101	11	of	of	ADP
eurjchem-1541	101	12	0.02	0.02	NUM
eurjchem-1541	101	13	m	m	NOUN
eurjchem-1541	101	14	sodium	sodium	NOUN
eurjchem-1541	101	15	phosphate	phosphate	NOUN
eurjchem-1541	101	16	buffer	buffer	NOUN
eurjchem-1541	101	17	(	(	PUNCT
eurjchem-1541	101	18	ph	ph	NOUN
eurjchem-1541	101	19	=	=	NOUN
eurjchem-1541	101	20	6.9	6.9	NUM
eurjchem-1541	101	21	)	)	PUNCT
eurjchem-1541	101	22	containing	contain	VERB
eurjchem-1541	101	23	α‐amylase	α‐amylase	NUM
eurjchem-1541	101	24	solution	solution	NOUN
eurjchem-1541	101	25	(	(	PUNCT
eurjchem-1541	101	26	240	240	NUM
eurjchem-1541	101	27	u	u	NOUN
eurjchem-1541	101	28	/	/	SYM
eurjchem-1541	101	29	ml	ml	VERB
eurjchem-1541	101	30	)	)	PUNCT
eurjchem-1541	101	31	were	be	AUX
eurjchem-1541	101	32	incubated	incubate	VERB
eurjchem-1541	101	33	at	at	ADP
eurjchem-1541	101	34	37	37	NUM
eurjchem-1541	101	35	°	°	NOUN
eurjchem-1541	101	36	c	c	NOUN
eurjchem-1541	101	37	for	for	ADP
eurjchem-1541	101	38	20	20	NUM
eurjchem-1541	101	39	minutes	minute	NOUN
eurjchem-1541	101	40	.	.	PUNCT
eurjchem-1541	102	1	after	after	ADP
eurjchem-1541	102	2	pre‐incubation	pre‐incubation	NOUN
eurjchem-1541	102	3	,	,	PUNCT
eurjchem-1541	102	4	250	250	NUM
eurjchem-1541	102	5	μl	μl	ADP
eurjchem-1541	102	6	of	of	ADP
eurjchem-1541	102	7	a	a	DET
eurjchem-1541	102	8	1	1	NUM
eurjchem-1541	102	9	%	%	NOUN
eurjchem-1541	102	10	starch	starch	NOUN
eurjchem-1541	102	11	solution	solution	NOUN
eurjchem-1541	102	12	in	in	ADP
eurjchem-1541	102	13	0.02	0.02	NUM
eurjchem-1541	102	14	m	m	NOUN
eurjchem-1541	102	15	sodium	sodium	NOUN
eurjchem-1541	102	16	phosphate	phosphate	NOUN
eurjchem-1541	102	17	buffer	buffer	NOUN
eurjchem-1541	102	18	(	(	PUNCT
eurjchem-1541	102	19	ph	ph	NOUN
eurjchem-1541	102	20	=	=	SYM
eurjchem-1541	102	21	6.7	6.7	NUM
eurjchem-1541	102	22	)	)	PUNCT
eurjchem-1541	102	23	was	be	AUX
eurjchem-1541	102	24	added	add	VERB
eurjchem-1541	102	25	to	to	ADP
eurjchem-1541	102	26	each	each	DET
eurjchem-1541	102	27	tube	tube	NOUN
eurjchem-1541	102	28	at	at	ADP
eurjchem-1541	102	29	timed	time	VERB
eurjchem-1541	102	30	intervals	interval	NOUN
eurjchem-1541	102	31	.	.	PUNCT
eurjchem-1541	103	1	the	the	DET
eurjchem-1541	103	2	reaction	reaction	NOUN
eurjchem-1541	103	3	mixtures	mixture	NOUN
eurjchem-1541	103	4	were	be	AUX
eurjchem-1541	103	5	then	then	ADV
eurjchem-1541	103	6	incubated	incubate	VERB
eurjchem-1541	103	7	at	at	ADP
eurjchem-1541	103	8	37	37	NUM
eurjchem-1541	103	9	°	°	NOUN
eurjchem-1541	103	10	c	c	NOUN
eurjchem-1541	103	11	for	for	ADP
eurjchem-1541	103	12	15	15	NUM
eurjchem-1541	103	13	minutes	minute	NOUN
eurjchem-1541	103	14	.	.	PUNCT
eurjchem-1541	104	1	the	the	DET
eurjchem-1541	104	2	reaction	reaction	NOUN
eurjchem-1541	104	3	was	be	AUX
eurjchem-1541	104	4	stopped	stop	VERB
eurjchem-1541	104	5	with	with	ADP
eurjchem-1541	104	6	1.0	1.0	NUM
eurjchem-1541	104	7	ml	ml	NOUN
eurjchem-1541	104	8	of	of	ADP
eurjchem-1541	104	9	dinitrosalicylic	dinitrosalicylic	ADJ
eurjchem-1541	104	10	acid	acid	NOUN
eurjchem-1541	104	11	color	color	NOUN
eurjchem-1541	104	12	reagent	reagent	NOUN
eurjchem-1541	104	13	.	.	PUNCT
eurjchem-1541	105	1	the	the	DET
eurjchem-1541	105	2	test	test	NOUN
eurjchem-1541	105	3	tubes	tube	NOUN
eurjchem-1541	105	4	were	be	AUX
eurjchem-1541	105	5	then	then	ADV
eurjchem-1541	105	6	incubated	incubate	VERB
eurjchem-1541	105	7	in	in	ADP
eurjchem-1541	105	8	a	a	DET
eurjchem-1541	105	9	boiling	boil	VERB
eurjchem-1541	105	10	water	water	NOUN
eurjchem-1541	105	11	bath	bath	NOUN
eurjchem-1541	105	12	for	for	ADP
eurjchem-1541	105	13	10	10	NUM
eurjchem-1541	105	14	minutes	minute	NOUN
eurjchem-1541	105	15	,	,	PUNCT
eurjchem-1541	105	16	cooled	cool	VERB
eurjchem-1541	105	17	to	to	ADP
eurjchem-1541	105	18	room	room	NOUN
eurjchem-1541	105	19	temperature	temperature	NOUN
eurjchem-1541	105	20	.	.	PUNCT
eurjchem-1541	106	1	the	the	DET
eurjchem-1541	106	2	reaction	reaction	NOUN
eurjchem-1541	106	3	mixture	mixture	NOUN
eurjchem-1541	106	4	was	be	AUX
eurjchem-1541	106	5	diluted	dilute	VERB
eurjchem-1541	106	6	after	after	ADP
eurjchem-1541	106	7	adding	add	VERB
eurjchem-1541	106	8	2	2	NUM
eurjchem-1541	106	9	ml	ml	NOUN
eurjchem-1541	106	10	of	of	ADP
eurjchem-1541	106	11	distilled	distil	VERB
eurjchem-1541	106	12	water	water	NOUN
eurjchem-1541	106	13	and	and	CCONJ
eurjchem-1541	106	14	absorbance	absorbance	NOUN
eurjchem-1541	106	15	was	be	AUX
eurjchem-1541	106	16	recorded	record	VERB
eurjchem-1541	106	17	at	at	ADP
eurjchem-1541	106	18	540	540	NUM
eurjchem-1541	106	19	nm	nm	NOUN
eurjchem-1541	106	20	using	use	VERB
eurjchem-1541	106	21	the	the	DET
eurjchem-1541	106	22	spectrophotometer	spectrophotometer	NOUN
eurjchem-1541	106	23	.	.	PUNCT
eurjchem-1541	107	1	2.5.2	2.5.2	NUM
eurjchem-1541	107	2	.	.	X
eurjchem-1541	107	3	α‐glucosidase	α‐glucosidase	PUNCT
eurjchem-1541	107	4	inhibitory	inhibitory	NOUN
eurjchem-1541	107	5	assay	assay	VERB
eurjchem-1541	107	6	‐glucosidase	‐glucosidase	ADJ
eurjchem-1541	107	7	inhibitory	inhibitory	ADJ
eurjchem-1541	107	8	activity	activity	NOUN
eurjchem-1541	107	9	of	of	ADP
eurjchem-1541	107	10	the	the	DET
eurjchem-1541	107	11	synthesized	synthesize	VERB
eurjchem-1541	107	12	compounds	compound	NOUN
eurjchem-1541	107	13	was	be	AUX
eurjchem-1541	107	14	determined	determine	VERB
eurjchem-1541	107	15	using	use	VERB
eurjchem-1541	107	16	the	the	DET
eurjchem-1541	107	17	substrate	substrate	NOUN
eurjchem-1541	107	18	pnpg	pnpg	NOUN
eurjchem-1541	107	19	according	accord	VERB
eurjchem-1541	107	20	to	to	ADP
eurjchem-1541	107	21	the	the	DET
eurjchem-1541	107	22	previously	previously	ADV
eurjchem-1541	107	23	reported	report	VERB
eurjchem-1541	107	24	method	method	NOUN
eurjchem-1541	107	25	[	[	X
eurjchem-1541	107	26	24	24	NUM
eurjchem-1541	107	27	]	]	PUNCT
eurjchem-1541	107	28	.	.	PUNCT
eurjchem-1541	108	1	a	a	DET
eurjchem-1541	108	2	volume	volume	NOUN
eurjchem-1541	108	3	of	of	ADP
eurjchem-1541	108	4	150	150	NUM
eurjchem-1541	108	5	μl	μl	ADP
eurjchem-1541	108	6	of	of	ADP
eurjchem-1541	108	7	sample	sample	NOUN
eurjchem-1541	108	8	solution	solution	NOUN
eurjchem-1541	108	9	and	and	CCONJ
eurjchem-1541	108	10	100	100	NUM
eurjchem-1541	108	11	μl	μl	ADP
eurjchem-1541	108	12	of	of	ADP
eurjchem-1541	108	13	0.1	0.1	NUM
eurjchem-1541	108	14	m	m	NOUN
eurjchem-1541	108	15	phosphate	phosphate	NOUN
eurjchem-1541	108	16	buffer	buffer	NOUN
eurjchem-1541	108	17	(	(	PUNCT
eurjchem-1541	108	18	ph	ph	NOUN
eurjchem-1541	108	19	=	=	SYM
eurjchem-1541	108	20	6.7	6.7	NUM
eurjchem-1541	108	21	)	)	PUNCT
eurjchem-1541	108	22	containing	contain	VERB
eurjchem-1541	108	23	α‐glucosidase	α‐glucosidase	NOUN
eurjchem-1541	108	24	solution	solution	NOUN
eurjchem-1541	108	25	(	(	PUNCT
eurjchem-1541	108	26	0.1	0.1	NUM
eurjchem-1541	108	27	u	u	NOUN
eurjchem-1541	108	28	/	/	SYM
eurjchem-1541	108	29	ml	ml	NOUN
eurjchem-1541	108	30	)	)	PUNCT
eurjchem-1541	108	31	was	be	AUX
eurjchem-1541	108	32	incubated	incubate	VERB
eurjchem-1541	108	33	at	at	ADP
eurjchem-1541	108	34	37	37	NUM
eurjchem-1541	108	35	°	°	NOUN
eurjchem-1541	108	36	c	c	NOUN
eurjchem-1541	108	37	for	for	ADP
eurjchem-1541	108	38	10	10	NUM
eurjchem-1541	108	39	minutes	minute	NOUN
eurjchem-1541	108	40	.	.	PUNCT
eurjchem-1541	109	1	after	after	ADP
eurjchem-1541	109	2	pre‐incubation	pre‐incubation	NOUN
eurjchem-1541	109	3	,	,	PUNCT
eurjchem-1541	109	4	200	200	NUM
eurjchem-1541	109	5	μl	μl	ADP
eurjchem-1541	109	6	of	of	ADP
eurjchem-1541	109	7	1	1	NUM
eurjchem-1541	109	8	mm	mm	NOUN
eurjchem-1541	109	9	p‐nitrophenyl‐α‐d‐glucopyranoside	p‐nitrophenyl‐α‐d‐glucopyranoside	NOUN
eurjchem-1541	109	10	solution	solution	NOUN
eurjchem-1541	109	11	in	in	ADP
eurjchem-1541	109	12	0.1	0.1	NUM
eurjchem-1541	109	13	m	m	NOUN
eurjchem-1541	109	14	phosphate	phosphate	NOUN
eurjchem-1541	109	15	buffer	buffer	NOUN
eurjchem-1541	109	16	(	(	PUNCT
eurjchem-1541	109	17	ph	ph	NOUN
eurjchem-1541	109	18	=	=	SYM
eurjchem-1541	109	19	6.7	6.7	NUM
eurjchem-1541	109	20	)	)	PUNCT
eurjchem-1541	109	21	were	be	AUX
eurjchem-1541	109	22	added	add	VERB
eurjchem-1541	109	23	.	.	PUNCT
eurjchem-1541	110	1	the	the	DET
eurjchem-1541	110	2	reaction	reaction	NOUN
eurjchem-1541	110	3	mixtures	mixture	NOUN
eurjchem-1541	110	4	were	be	AUX
eurjchem-1541	110	5	incubated	incubate	VERB
eurjchem-1541	110	6	at	at	ADP
eurjchem-1541	110	7	37	37	NUM
eurjchem-1541	110	8	°	°	NOUN
eurjchem-1541	110	9	c	c	NOUN
eurjchem-1541	110	10	for	for	ADP
eurjchem-1541	110	11	30	30	NUM
eurjchem-1541	110	12	minutes	minute	NOUN
eurjchem-1541	110	13	.	.	PUNCT
eurjchem-1541	111	1	after	after	ADP
eurjchem-1541	111	2	incubation	incubation	NOUN
eurjchem-1541	111	3	,	,	PUNCT
eurjchem-1541	111	4	1	1	NUM
eurjchem-1541	111	5	ml	ml	NOUN
eurjchem-1541	111	6	of	of	ADP
eurjchem-1541	111	7	0.1	0.1	NUM
eurjchem-1541	111	8	m	m	NOUN
eurjchem-1541	111	9	of	of	ADP
eurjchem-1541	111	10	na2co3	na2co3	PROPN
eurjchem-1541	111	11	was	be	AUX
eurjchem-1541	111	12	added	add	VERB
eurjchem-1541	111	13	and	and	CCONJ
eurjchem-1541	111	14	the	the	DET
eurjchem-1541	111	15	absorbance	absorbance	NOUN
eurjchem-1541	111	16	was	be	AUX
eurjchem-1541	111	17	measured	measure	VERB
eurjchem-1541	111	18	at	at	ADP
eurjchem-1541	111	19	405	405	NUM
eurjchem-1541	111	20	nm	nm	NOUN
eurjchem-1541	111	21	in	in	ADP
eurjchem-1541	111	22	the	the	DET
eurjchem-1541	111	23	spectrophoto‐	spectrophoto‐	NOUN
eurjchem-1541	111	24	meter	meter	NOUN
eurjchem-1541	111	25	.	.	PUNCT
eurjchem-1541	112	1	the	the	PRON
eurjchem-1541	112	2	α‐glucosidase	α‐glucosidase	PUNCT
eurjchem-1541	112	3	and	and	CCONJ
eurjchem-1541	112	4	α‐amylase	α‐amylase	PUNCT
eurjchem-1541	112	5	inhibitory	inhibitory	ADJ
eurjchem-1541	112	6	activity	activity	NOUN
eurjchem-1541	112	7	were	be	AUX
eurjchem-1541	112	8	expressed	express	VERB
eurjchem-1541	112	9	as	as	ADP
eurjchem-1541	112	10	percentage	percentage	NOUN
eurjchem-1541	112	11	inhibition	inhibition	NOUN
eurjchem-1541	112	12	and	and	CCONJ
eurjchem-1541	112	13	the	the	DET
eurjchem-1541	112	14	concent‐	concent‐	NOUN
eurjchem-1541	112	15	rations	ration	NOUN
eurjchem-1541	112	16	of	of	ADP
eurjchem-1541	112	17	tested	test	VERB
eurjchem-1541	112	18	compounds	compound	NOUN
eurjchem-1541	112	19	required	require	VERB
eurjchem-1541	112	20	to	to	PART
eurjchem-1541	112	21	inhibit	inhibit	VERB
eurjchem-1541	112	22	50	50	NUM
eurjchem-1541	112	23	%	%	NOUN
eurjchem-1541	112	24	of	of	ADP
eurjchem-1541	112	25	enzymes	enzyme	NOUN
eurjchem-1541	112	26	activity	activity	NOUN
eurjchem-1541	112	27	(	(	PUNCT
eurjchem-1541	112	28	ic50	ic50	PROPN
eurjchem-1541	112	29	)	)	PUNCT
eurjchem-1541	112	30	were	be	AUX
eurjchem-1541	112	31	determined	determine	VERB
eurjchem-1541	112	32	.	.	PUNCT
eurjchem-1541	113	1	acarbose	acarbose	PROPN
eurjchem-1541	113	2	was	be	AUX
eurjchem-1541	113	3	used	use	VERB
eurjchem-1541	113	4	as	as	ADP
eurjchem-1541	113	5	reference	reference	NOUN
eurjchem-1541	113	6	standard	standard	NOUN
eurjchem-1541	113	7	.	.	PUNCT
eurjchem-1541	114	1	3	3	X
eurjchem-1541	114	2	.	.	NOUN
eurjchem-1541	114	3	results	result	NOUN
eurjchem-1541	114	4	and	and	CCONJ
eurjchem-1541	114	5	discussion	discussion	NOUN
eurjchem-1541	114	6	3.1	3.1	NUM
eurjchem-1541	114	7	.	.	PUNCT
eurjchem-1541	115	1	synthesis	synthesis	NOUN
eurjchem-1541	115	2	treatment	treatment	NOUN
eurjchem-1541	115	3	of	of	ADP
eurjchem-1541	115	4	1h‐pyrazolo[3,4‐d]pyrimidin‐4(5h)‐one	1h‐pyrazolo[3,4‐d]pyrimidin‐4(5h)‐one	PROPN
eurjchem-1541	115	5	(	(	PUNCT
eurjchem-1541	115	6	a	a	NOUN
eurjchem-1541	115	7	)	)	PUNCT
eurjchem-1541	115	8	in	in	ADP
eurjchem-1541	115	9	absolute	absolute	ADJ
eurjchem-1541	115	10	ethanol	ethanol	NOUN
eurjchem-1541	115	11	with	with	ADP
eurjchem-1541	115	12	phosphorus	phosphorus	NOUN
eurjchem-1541	115	13	pentasulfide	pentasulfide	NOUN
eurjchem-1541	115	14	afforded	afford	VERB
eurjchem-1541	115	15	the	the	DET
eurjchem-1541	115	16	corresponding	correspond	VERB
eurjchem-1541	115	17	pyrazolo[3,4‐d]pyrimidine‐4‐thione	pyrazolo[3,4‐d]pyrimidine‐4‐thione	PROPN
eurjchem-1541	115	18	(	(	PUNCT
eurjchem-1541	115	19	b	b	NOUN
eurjchem-1541	115	20	)	)	PUNCT
eurjchem-1541	115	21	,	,	PUNCT
eurjchem-1541	115	22	with	with	ADP
eurjchem-1541	115	23	yield	yield	NOUN
eurjchem-1541	115	24	of	of	ADP
eurjchem-1541	115	25	90	90	NUM
eurjchem-1541	115	26	%	%	NOUN
eurjchem-1541	115	27	(	(	PUNCT
eurjchem-1541	115	28	scheme	scheme	NOUN
eurjchem-1541	115	29	1	1	NUM
eurjchem-1541	115	30	)	)	PUNCT
eurjchem-1541	115	31	.	.	PUNCT
eurjchem-1541	116	1	the	the	DET
eurjchem-1541	116	2	structure	structure	NOUN
eurjchem-1541	116	3	of	of	ADP
eurjchem-1541	116	4	sulfur	sulfur	NOUN
eurjchem-1541	116	5	product	product	NOUN
eurjchem-1541	116	6	b	b	PROPN
eurjchem-1541	116	7	was	be	AUX
eurjchem-1541	116	8	elucidated	elucidate	VERB
eurjchem-1541	116	9	by	by	ADP
eurjchem-1541	116	10	mass	mass	NOUN
eurjchem-1541	116	11	spectrum	spectrum	NOUN
eurjchem-1541	116	12	of	of	ADP
eurjchem-1541	116	13	the	the	DET
eurjchem-1541	116	14	compound	compound	PROPN
eurjchem-1541	116	15	b	b	PROPN
eurjchem-1541	116	16	,	,	PUNCT
eurjchem-1541	116	17	taken	take	VERB
eurjchem-1541	116	18	in	in	ADP
eurjchem-1541	116	19	electronic	electronic	ADJ
eurjchem-1541	116	20	impact	impact	NOUN
eurjchem-1541	116	21	mode	mode	NOUN
eurjchem-1541	116	22	,	,	PUNCT
eurjchem-1541	116	23	indicates	indicate	VERB
eurjchem-1541	116	24	a	a	DET
eurjchem-1541	116	25	molecular	molecular	ADJ
eurjchem-1541	116	26	peak	peak	NOUN
eurjchem-1541	116	27	at	at	ADP
eurjchem-1541	116	28	m	m	PROPN
eurjchem-1541	116	29	/	/	SYM
eurjchem-1541	116	30	z	z	NOUN
eurjchem-1541	116	31	152	152	NUM
eurjchem-1541	117	1	[	[	X
eurjchem-1541	117	2	m+	m+	NOUN
eurjchem-1541	117	3	]	]	PUNCT
eurjchem-1541	117	4	.	.	PUNCT
eurjchem-1541	118	1	the	the	DET
eurjchem-1541	118	2	action	action	NOUN
eurjchem-1541	118	3	of	of	ADP
eurjchem-1541	118	4	one	one	NUM
eurjchem-1541	118	5	equivalent	equivalent	NOUN
eurjchem-1541	118	6	of	of	ADP
eurjchem-1541	118	7	the	the	DET
eurjchem-1541	118	8	various	various	ADJ
eurjchem-1541	118	9	alkylating	alkylate	VERB
eurjchem-1541	118	10	agents	agent	NOUN
eurjchem-1541	118	11	(	(	PUNCT
eurjchem-1541	118	12	allyl	allyl	NOUN
eurjchem-1541	118	13	chloride	chloride	NOUN
eurjchem-1541	118	14	,	,	PUNCT
eurjchem-1541	118	15	propargyl	propargyl	PROPN
eurjchem-1541	118	16	chloride	chloride	NOUN
eurjchem-1541	118	17	,	,	PUNCT
eurjchem-1541	118	18	benzyl	benzyl	NOUN
eurjchem-1541	118	19	chloride	chloride	NOUN
eurjchem-1541	118	20	)	)	PUNCT
eurjchem-1541	118	21	on	on	ADP
eurjchem-1541	118	22	the	the	DET
eurjchem-1541	118	23	pyrazolo	pyrazolo	NOUN
eurjchem-1541	119	1	[	[	X
eurjchem-1541	119	2	3,4‐d	3,4‐d	NOUN
eurjchem-1541	119	3	]	]	PUNCT
eurjchem-1541	119	4	pyrimidine‐4	pyrimidine‐4	X
eurjchem-1541	119	5	(	(	PUNCT
eurjchem-1541	119	6	5h)‐thione	5h)‐thione	NUM
eurjchem-1541	119	7	in	in	ADP
eurjchem-1541	119	8	dmf	dmf	PROPN
eurjchem-1541	119	9	for	for	ADP
eurjchem-1541	119	10	48	48	NUM
eurjchem-1541	119	11	hours	hour	NOUN
eurjchem-1541	119	12	under	under	ADP
eurjchem-1541	119	13	conditions	condition	NOUN
eurjchem-1541	119	14	of	of	ADP
eurjchem-1541	119	15	the	the	DET
eurjchem-1541	119	16	phase	phase	NOUN
eurjchem-1541	119	17	transfer	transfer	NOUN
eurjchem-1541	119	18	catalysis	catalysis	NOUN
eurjchem-1541	119	19	(	(	PUNCT
eurjchem-1541	119	20	ctp	ctp	PROPN
eurjchem-1541	119	21	)	)	PUNCT
eurjchem-1541	119	22	using	use	VERB
eurjchem-1541	119	23	btba	btba	NOUN
eurjchem-1541	119	24	as	as	ADP
eurjchem-1541	119	25	the	the	DET
eurjchem-1541	119	26	catalyst	catalyst	NOUN
eurjchem-1541	119	27	and	and	CCONJ
eurjchem-1541	119	28	the	the	DET
eurjchem-1541	119	29	carbonate	carbonate	NOUN
eurjchem-1541	119	30	potassium	potassium	NOUN
eurjchem-1541	119	31	as	as	ADP
eurjchem-1541	119	32	a	a	DET
eurjchem-1541	119	33	base	base	NOUN
eurjchem-1541	119	34	[	[	X
eurjchem-1541	119	35	10,11	10,11	NOUN
eurjchem-1541	119	36	]	]	PUNCT
eurjchem-1541	119	37	,	,	PUNCT
eurjchem-1541	119	38	allows	allow	VERB
eurjchem-1541	119	39	the	the	DET
eurjchem-1541	119	40	exclusive	exclusive	ADJ
eurjchem-1541	119	41	alkylation	alkylation	NOUN
eurjchem-1541	119	42	of	of	ADP
eurjchem-1541	119	43	the	the	DET
eurjchem-1541	119	44	sulfur	sulfur	NOUN
eurjchem-1541	119	45	atom	atom	NOUN
eurjchem-1541	119	46	and	and	CCONJ
eurjchem-1541	119	47	thus	thus	ADV
eurjchem-1541	119	48	leads	lead	VERB
eurjchem-1541	119	49	to	to	ADP
eurjchem-1541	119	50	formation	formation	NOUN
eurjchem-1541	119	51	of	of	ADP
eurjchem-1541	119	52	the	the	DET
eurjchem-1541	119	53	s‐alkylation	s‐alkylation	PUNCT
eurjchem-1541	119	54	product	product	NOUN
eurjchem-1541	119	55	with	with	ADP
eurjchem-1541	119	56	a	a	DET
eurjchem-1541	119	57	yield	yield	NOUN
eurjchem-1541	119	58	of	of	ADP
eurjchem-1541	119	59	65	65	NUM
eurjchem-1541	119	60	%	%	NOUN
eurjchem-1541	119	61	(	(	PUNCT
eurjchem-1541	119	62	scheme	scheme	NOUN
eurjchem-1541	119	63	2	2	NUM
eurjchem-1541	119	64	)	)	PUNCT
eurjchem-1541	119	65	.	.	PUNCT
eurjchem-1541	120	1	the	the	DET
eurjchem-1541	120	2	structures	structure	NOUN
eurjchem-1541	120	3	of	of	ADP
eurjchem-1541	120	4	compounds	compound	NOUN
eurjchem-1541	120	5	c‐e	c‐e	VERB
eurjchem-1541	120	6	were	be	AUX
eurjchem-1541	120	7	determined	determine	VERB
eurjchem-1541	120	8	by	by	ADP
eurjchem-1541	120	9	spectroscopic	spectroscopic	ADJ
eurjchem-1541	120	10	methods	method	NOUN
eurjchem-1541	120	11	.	.	PUNCT
eurjchem-1541	121	1	the	the	DET
eurjchem-1541	121	2	1h	1h	NUM
eurjchem-1541	121	3	nmr	nmr	NOUN
eurjchem-1541	121	4	spectra	spectra	ADJ
eurjchem-1541	121	5	show	show	NOUN
eurjchem-1541	121	6	,	,	PUNCT
eurjchem-1541	121	7	in	in	ADP
eurjchem-1541	121	8	particular	particular	ADJ
eurjchem-1541	121	9	,	,	PUNCT
eurjchem-1541	121	10	the	the	DET
eurjchem-1541	121	11	signals	signal	NOUN
eurjchem-1541	121	12	relating	relate	VERB
eurjchem-1541	121	13	to	to	ADP
eurjchem-1541	121	14	the	the	DET
eurjchem-1541	121	15	alkyl	alkyl	ADJ
eurjchem-1541	121	16	groups	group	NOUN
eurjchem-1541	121	17	,	,	PUNCT
eurjchem-1541	121	18	as	as	ADV
eurjchem-1541	121	19	well	well	ADV
eurjchem-1541	121	20	as	as	ADP
eurjchem-1541	121	21	the	the	DET
eurjchem-1541	121	22	signals	signal	NOUN
eurjchem-1541	121	23	relating	relate	VERB
eurjchem-1541	121	24	to	to	ADP
eurjchem-1541	121	25	the	the	DET
eurjchem-1541	121	26	protons	proton	NOUN
eurjchem-1541	121	27	h3	h3	NOUN
eurjchem-1541	121	28	and	and	CCONJ
eurjchem-1541	121	29	h6	h6	PROPN
eurjchem-1541	121	30	of	of	ADP
eurjchem-1541	121	31	the	the	DET
eurjchem-1541	121	32	bicyclic	bicyclic	NOUN
eurjchem-1541	121	33	system	system	NOUN
eurjchem-1541	121	34	.	.	PUNCT
eurjchem-1541	122	1	the	the	DET
eurjchem-1541	122	2	13	13	NUM
eurjchem-1541	122	3	c	c	PROPN
eurjchem-1541	122	4	nmr	nmr	NOUN
eurjchem-1541	122	5	spectra	spectra	NOUN
eurjchem-1541	122	6	show	show	VERB
eurjchem-1541	122	7	the	the	DET
eurjchem-1541	122	8	signals	signal	NOUN
eurjchem-1541	122	9	relative	relative	ADJ
eurjchem-1541	122	10	to	to	ADP
eurjchem-1541	122	11	the	the	DET
eurjchem-1541	122	12	carbons	carbon	NOUN
eurjchem-1541	122	13	of	of	ADP
eurjchem-1541	122	14	the	the	DET
eurjchem-1541	122	15	alkyl	alkyl	ADJ
eurjchem-1541	122	16	groups	group	NOUN
eurjchem-1541	122	17	carried	carry	VERB
eurjchem-1541	122	18	by	by	ADP
eurjchem-1541	122	19	the	the	DET
eurjchem-1541	122	20	sulfur	sulfur	NOUN
eurjchem-1541	122	21	atom	atom	NOUN
eurjchem-1541	122	22	.	.	PUNCT
eurjchem-1541	123	1	an	an	DET
eurjchem-1541	123	2	x‐ray	x‐ray	PROPN
eurjchem-1541	123	3	diffraction	diffraction	NOUN
eurjchem-1541	123	4	study	study	NOUN
eurjchem-1541	123	5	confirmed	confirm	VERB
eurjchem-1541	123	6	the	the	DET
eurjchem-1541	123	7	proposed	propose	VERB
eurjchem-1541	123	8	structure	structure	NOUN
eurjchem-1541	123	9	,	,	PUNCT
eurjchem-1541	123	10	previously	previously	ADV
eurjchem-1541	123	11	on	on	ADP
eurjchem-1541	123	12	the	the	DET
eurjchem-1541	123	13	basis	basis	NOUN
eurjchem-1541	123	14	of	of	ADP
eurjchem-1541	123	15	the	the	DET
eurjchem-1541	123	16	nmr	nmr	NOUN
eurjchem-1541	123	17	spectra	spectra	NOUN
eurjchem-1541	123	18	of	of	ADP
eurjchem-1541	123	19	compounds	compound	NOUN
eurjchem-1541	123	20	c	c	PROPN
eurjchem-1541	123	21	and	and	CCONJ
eurjchem-1541	123	22	e	e	X
eurjchem-1541	124	1	[	[	X
eurjchem-1541	124	2	15,16	15,16	NUM
eurjchem-1541	124	3	]	]	PUNCT
eurjchem-1541	124	4	.	.	PUNCT
eurjchem-1541	125	1	1,3‐dipolar	1,3‐dipolar	NUM
eurjchem-1541	125	2	cycloaddition	cycloaddition	NOUN
eurjchem-1541	125	3	is	be	AUX
eurjchem-1541	125	4	a	a	DET
eurjchem-1541	125	5	method	method	NOUN
eurjchem-1541	125	6	of	of	ADP
eurjchem-1541	125	7	synthesis	synthesis	NOUN
eurjchem-1541	125	8	of	of	ADP
eurjchem-1541	125	9	five	five	NUM
eurjchem-1541	125	10	membered	membere	VERB
eurjchem-1541	125	11	heterocycles	heterocycle	NOUN
eurjchem-1541	125	12	,	,	PUNCT
eurjchem-1541	125	13	which	which	PRON
eurjchem-1541	125	14	are	be	AUX
eurjchem-1541	125	15	difficult	difficult	ADJ
eurjchem-1541	125	16	to	to	PART
eurjchem-1541	125	17	prepare	prepare	VERB
eurjchem-1541	125	18	by	by	ADP
eurjchem-1541	125	19	other	other	ADJ
eurjchem-1541	125	20	means	mean	NOUN
eurjchem-1541	125	21	.	.	PUNCT
eurjchem-1541	126	1	interestingly	interestingly	ADV
eurjchem-1541	126	2	,	,	PUNCT
eurjchem-1541	126	3	condensation	condensation	NOUN
eurjchem-1541	126	4	reaction	reaction	NOUN
eurjchem-1541	126	5	of	of	ADP
eurjchem-1541	126	6	arylnitrile	arylnitrile	ADJ
eurjchem-1541	126	7	108	108	NUM
eurjchem-1541	126	8	el‐fal	el‐fal	NOUN
eurjchem-1541	126	9	et	et	NOUN
eurjchem-1541	126	10	al	al	PROPN
eurjchem-1541	126	11	.	.	PUNCT
eurjchem-1541	126	12	/	/	SYM
eurjchem-1541	126	13	european	european	PROPN
eurjchem-1541	126	14	journal	journal	PROPN
eurjchem-1541	126	15	of	of	ADP
eurjchem-1541	126	16	chemistry	chemistry	NOUN
eurjchem-1541	126	17	8	8	NUM
eurjchem-1541	126	18	(	(	PUNCT
eurjchem-1541	126	19	2	2	NUM
eurjchem-1541	126	20	)	)	PUNCT
eurjchem-1541	126	21	(	(	PUNCT
eurjchem-1541	126	22	2017	2017	NUM
eurjchem-1541	126	23	)	)	PUNCT
eurjchem-1541	126	24	105‐108	105‐108	NUM
eurjchem-1541	126	25	oxide	oxide	NOUN
eurjchem-1541	126	26	,	,	PUNCT
eurjchem-1541	126	27	prepared	prepare	VERB
eurjchem-1541	126	28	in	in	ADP
eurjchem-1541	126	29	situ	situ	NOUN
eurjchem-1541	126	30	by	by	ADP
eurjchem-1541	126	31	the	the	DET
eurjchem-1541	126	32	action	action	NOUN
eurjchem-1541	126	33	of	of	ADP
eurjchem-1541	126	34	water	water	NOUN
eurjchem-1541	126	35	of	of	ADP
eurjchem-1541	126	36	javel	javel	NOUN
eurjchem-1541	126	37	on	on	ADP
eurjchem-1541	126	38	benzaldehyde	benzaldehyde	NOUN
eurjchem-1541	126	39	oxime	oxime	NOUN
eurjchem-1541	126	40	,	,	PUNCT
eurjchem-1541	126	41	with	with	ADP
eurjchem-1541	126	42	propargylpyrazolo[3,4‐d]pyrimi‐	propargylpyrazolo[3,4‐d]pyrimi‐	PROPN
eurjchem-1541	126	43	dine	dine	PROPN
eurjchem-1541	126	44	d	d	PROPN
eurjchem-1541	126	45	in	in	ADP
eurjchem-1541	126	46	a	a	DET
eurjchem-1541	126	47	two‐phase	two‐phase	NOUN
eurjchem-1541	126	48	medium	medium	ADJ
eurjchem-1541	126	49	(	(	PUNCT
eurjchem-1541	126	50	water	water	NOUN
eurjchem-1541	126	51	/	/	SYM
eurjchem-1541	126	52	chloroform	chloroform	NOUN
eurjchem-1541	126	53	)	)	PUNCT
eurjchem-1541	126	54	at	at	ADP
eurjchem-1541	126	55	0	0	NUM
eurjchem-1541	126	56	°	°	ADP
eurjchem-1541	126	57	c	c	NOUN
eurjchem-1541	126	58	for	for	ADP
eurjchem-1541	126	59	2	2	NUM
eurjchem-1541	126	60	hours	hour	NOUN
eurjchem-1541	126	61	.	.	PUNCT
eurjchem-1541	127	1	it	it	PRON
eurjchem-1541	127	2	leads	lead	VERB
eurjchem-1541	127	3	exclusively	exclusively	ADV
eurjchem-1541	127	4	to	to	PART
eurjchem-1541	127	5	cycloadducts	cycloadduct	NOUN
eurjchem-1541	127	6	f	f	PROPN
eurjchem-1541	127	7	and	and	CCONJ
eurjchem-1541	127	8	g	g	PROPN
eurjchem-1541	127	9	(	(	PUNCT
eurjchem-1541	127	10	scheme	scheme	NOUN
eurjchem-1541	127	11	3	3	NUM
eurjchem-1541	127	12	)	)	PUNCT
eurjchem-1541	127	13	.	.	PUNCT
eurjchem-1541	128	1	the	the	DET
eurjchem-1541	128	2	structures	structure	NOUN
eurjchem-1541	128	3	of	of	ADP
eurjchem-1541	128	4	these	these	DET
eurjchem-1541	128	5	cycloadducts	cycloadduct	NOUN
eurjchem-1541	128	6	were	be	AUX
eurjchem-1541	128	7	elucidated	elucidate	VERB
eurjchem-1541	128	8	on	on	ADP
eurjchem-1541	128	9	the	the	DET
eurjchem-1541	128	10	basis	basis	NOUN
eurjchem-1541	128	11	of	of	ADP
eurjchem-1541	128	12	the	the	DET
eurjchem-1541	128	13	nmr	nmr	NOUN
eurjchem-1541	128	14	spectral	spectral	ADJ
eurjchem-1541	128	15	data	data	PROPN
eurjchem-1541	128	16	,	,	PUNCT
eurjchem-1541	128	17	ir	ir	PROPN
eurjchem-1541	128	18	,	,	PUNCT
eurjchem-1541	128	19	and	and	CCONJ
eurjchem-1541	129	1	ms	ms	PROPN
eurjchem-1541	129	2	.	.	PROPN
eurjchem-1541	130	1	the	the	DET
eurjchem-1541	130	2	1h	1h	NUM
eurjchem-1541	130	3	nmr	nmr	NOUN
eurjchem-1541	130	4	of	of	ADP
eurjchem-1541	130	5	the	the	DET
eurjchem-1541	130	6	compound	compound	NOUN
eurjchem-1541	130	7	f	f	NOUN
eurjchem-1541	130	8	,	,	PUNCT
eurjchem-1541	130	9	essentially	essentially	ADV
eurjchem-1541	130	10	reveals	reveal	VERB
eurjchem-1541	130	11	the	the	DET
eurjchem-1541	130	12	presence	presence	NOUN
eurjchem-1541	130	13	of	of	ADP
eurjchem-1541	130	14	a	a	DET
eurjchem-1541	130	15	multiplet	multiplet	NOUN
eurjchem-1541	130	16	at	at	ADP
eurjchem-1541	130	17	δ	δ	PROPN
eurjchem-1541	130	18	4.52	4.52	NUM
eurjchem-1541	130	19	ppm	ppm	NOUN
eurjchem-1541	130	20	,	,	PUNCT
eurjchem-1541	130	21	due	due	ADP
eurjchem-1541	130	22	to	to	ADP
eurjchem-1541	130	23	the	the	DET
eurjchem-1541	130	24	sch2	sch2	PROPN
eurjchem-1541	130	25	group	group	NOUN
eurjchem-1541	130	26	,	,	PUNCT
eurjchem-1541	130	27	and	and	CCONJ
eurjchem-1541	130	28	a	a	DET
eurjchem-1541	130	29	signal	signal	NOUN
eurjchem-1541	130	30	at	at	ADP
eurjchem-1541	130	31	δ	δ	PROPN
eurjchem-1541	130	32	6.53	6.53	NUM
eurjchem-1541	130	33	ppm	ppm	NOUN
eurjchem-1541	130	34	due	due	ADP
eurjchem-1541	130	35	to	to	ADP
eurjchem-1541	130	36	isoxazoline	isoxazoline	NOUN
eurjchem-1541	130	37	ch	ch	NOUN
eurjchem-1541	130	38	and	and	CCONJ
eurjchem-1541	130	39	13c	13c	NOUN
eurjchem-1541	130	40	nmr	nmr	NOUN
eurjchem-1541	130	41	signal	signal	NOUN
eurjchem-1541	130	42	at	at	ADP
eurjchem-1541	130	43	δ	δ	PROPN
eurjchem-1541	130	44	99.03	99.03	NUM
eurjchem-1541	130	45	ppm	ppm	NOUN
eurjchem-1541	130	46	.	.	PUNCT
eurjchem-1541	130	47	examining	examine	VERB
eurjchem-1541	130	48	the	the	DET
eurjchem-1541	130	49	1h	1h	NUM
eurjchem-1541	130	50	nmr	nmr	NOUN
eurjchem-1541	130	51	of	of	ADP
eurjchem-1541	130	52	cycloadduct	cycloadduct	NOUN
eurjchem-1541	130	53	g	g	PROPN
eurjchem-1541	130	54	,	,	PUNCT
eurjchem-1541	130	55	one	one	NUM
eurjchem-1541	130	56	notices	notice	NOUN
eurjchem-1541	130	57	in	in	ADP
eurjchem-1541	130	58	particular	particular	ADJ
eurjchem-1541	130	59	the	the	DET
eurjchem-1541	130	60	appearance	appearance	NOUN
eurjchem-1541	130	61	of	of	ADP
eurjchem-1541	130	62	multiplet	multiplet	NOUN
eurjchem-1541	130	63	at	at	ADP
eurjchem-1541	130	64	δ	δ	PROPN
eurjchem-1541	130	65	4.03	4.03	NUM
eurjchem-1541	130	66	ppm	ppm	NOUN
eurjchem-1541	130	67	assigned	assign	VERB
eurjchem-1541	130	68	to	to	ADP
eurjchem-1541	130	69	the	the	DET
eurjchem-1541	130	70	sch2	sch2	PROPN
eurjchem-1541	130	71	group	group	NOUN
eurjchem-1541	130	72	.	.	PUNCT
eurjchem-1541	131	1	isoxazolinic	isoxazolinic	PROPN
eurjchem-1541	131	2	ch	ch	PROPN
eurjchem-1541	131	3	appears	appear	VERB
eurjchem-1541	131	4	as	as	ADP
eurjchem-1541	131	5	of	of	ADP
eurjchem-1541	131	6	a	a	DET
eurjchem-1541	131	7	signal	signal	NOUN
eurjchem-1541	131	8	which	which	PRON
eurjchem-1541	131	9	resonates	resonate	VERB
eurjchem-1541	131	10	at	at	ADP
eurjchem-1541	131	11	δ	δ	PROPN
eurjchem-1541	131	12	6.03	6.03	NUM
eurjchem-1541	131	13	ppm	ppm	NOUN
eurjchem-1541	131	14	and	and	CCONJ
eurjchem-1541	131	15	is	be	AUX
eurjchem-1541	131	16	manifested	manifest	VERB
eurjchem-1541	131	17	in	in	ADP
eurjchem-1541	131	18	13c	13c	NOUN
eurjchem-1541	131	19	nmr	nmr	NOUN
eurjchem-1541	131	20	by	by	ADP
eurjchem-1541	131	21	the	the	DET
eurjchem-1541	131	22	presence	presence	NOUN
eurjchem-1541	131	23	of	of	ADP
eurjchem-1541	131	24	a	a	DET
eurjchem-1541	131	25	signal	signal	NOUN
eurjchem-1541	131	26	at	at	ADP
eurjchem-1541	131	27	δ	δ	PROPN
eurjchem-1541	131	28	100.97	100.97	NUM
eurjchem-1541	131	29	ppm	ppm	NOUN
eurjchem-1541	131	30	.	.	PUNCT
eurjchem-1541	132	1	on	on	ADP
eurjchem-1541	132	2	the	the	DET
eurjchem-1541	132	3	ir	ir	PROPN
eurjchem-1541	132	4	spectrum	spectrum	NOUN
eurjchem-1541	132	5	of	of	ADP
eurjchem-1541	132	6	pure	pure	ADJ
eurjchem-1541	132	7	isolated	isolated	ADJ
eurjchem-1541	132	8	products	product	NOUN
eurjchem-1541	132	9	,	,	PUNCT
eurjchem-1541	132	10	the	the	DET
eurjchem-1541	132	11	presence	presence	NOUN
eurjchem-1541	132	12	of	of	ADP
eurjchem-1541	132	13	a	a	DET
eurjchem-1541	132	14	strong	strong	ADJ
eurjchem-1541	132	15	absorption	absorption	NOUN
eurjchem-1541	132	16	in	in	ADP
eurjchem-1541	132	17	the	the	DET
eurjchem-1541	132	18	zone	zone	NOUN
eurjchem-1541	132	19	1618‐1646	1618‐1646	PROPN
eurjchem-1541	132	20	cm‐1	cm‐1	PROPN
eurjchem-1541	132	21	corresponding	correspond	VERB
eurjchem-1541	132	22	to	to	ADP
eurjchem-1541	132	23	the	the	DET
eurjchem-1541	132	24	alkene	alkene	NOUN
eurjchem-1541	132	25	function	function	NOUN
eurjchem-1541	132	26	νc	νc	NOUN
eurjchem-1541	132	27	=	=	SYM
eurjchem-1541	132	28	c	c	NOUN
eurjchem-1541	132	29	and	and	CCONJ
eurjchem-1541	132	30	νc	νc	X
eurjchem-1541	132	31	=	=	NOUN
eurjchem-1541	132	32	n	n	NUM
eurjchem-1541	132	33	for	for	ADP
eurjchem-1541	132	34	1557cm‐1	1557cm‐1	NUM
eurjchem-1541	132	35	,	,	PUNCT
eurjchem-1541	132	36	at	at	ADP
eurjchem-1541	132	37	1212	1212	NUM
eurjchem-1541	132	38	cm‐1	cm‐1	NOUN
eurjchem-1541	132	39	corresponding	correspond	VERB
eurjchem-1541	132	40	to	to	ADP
eurjchem-1541	132	41	νc‐o	νc‐o	PROPN
eurjchem-1541	132	42	and	and	CCONJ
eurjchem-1541	132	43	νc‐n	νc‐n	NOUN
eurjchem-1541	132	44	around	around	ADP
eurjchem-1541	132	45	841‐936	841‐936	NUM
eurjchem-1541	132	46	cm‐1	cm‐1	NOUN
eurjchem-1541	132	47	.	.	PUNCT
eurjchem-1541	133	1	these	these	PRON
eurjchem-1541	133	2	are	be	AUX
eurjchem-1541	133	3	the	the	DET
eurjchem-1541	133	4	bands	band	NOUN
eurjchem-1541	133	5	charac‐	charac‐	PROPN
eurjchem-1541	133	6	teristic	teristic	NOUN
eurjchem-1541	133	7	of	of	ADP
eurjchem-1541	133	8	the	the	DET
eurjchem-1541	133	9	isoxazole	isoxazole	NOUN
eurjchem-1541	133	10	ring	ring	NOUN
eurjchem-1541	133	11	.	.	PUNCT
eurjchem-1541	134	1	3.2	3.2	NUM
eurjchem-1541	134	2	.	.	PUNCT
eurjchem-1541	134	3	in‐vitro	in‐vitro	VERB
eurjchem-1541	134	4	α‐amylase	α‐amylase	NUM
eurjchem-1541	134	5	and	and	CCONJ
eurjchem-1541	134	6	α‐glucosidase	α‐glucosidase	X
eurjchem-1541	134	7	inhibitory	inhibitory	ADJ
eurjchem-1541	134	8	activity	activity	NOUN
eurjchem-1541	134	9	the	the	DET
eurjchem-1541	134	10	inhibitory	inhibitory	ADJ
eurjchem-1541	134	11	activity	activity	NOUN
eurjchem-1541	134	12	of	of	ADP
eurjchem-1541	134	13	the	the	DET
eurjchem-1541	134	14	synthesized	synthesize	VERB
eurjchem-1541	134	15	compounds	compound	NOUN
eurjchem-1541	134	16	against	against	ADP
eurjchem-1541	134	17	α‐amylase	α‐amylase	NUM
eurjchem-1541	134	18	and	and	CCONJ
eurjchem-1541	134	19	α‐glucosidase	α‐glucosidase	NUM
eurjchem-1541	134	20	was	be	AUX
eurjchem-1541	134	21	measured	measure	VERB
eurjchem-1541	134	22	spectro‐	spectro‐	NOUN
eurjchem-1541	134	23	photometrically	photometrically	ADV
eurjchem-1541	134	24	.	.	PUNCT
eurjchem-1541	135	1	the	the	DET
eurjchem-1541	135	2	results	result	NOUN
eurjchem-1541	135	3	are	be	AUX
eurjchem-1541	135	4	shown	show	VERB
eurjchem-1541	135	5	in	in	ADP
eurjchem-1541	135	6	table	table	NOUN
eurjchem-1541	135	7	1	1	NUM
eurjchem-1541	135	8	.	.	PUNCT
eurjchem-1541	136	1	our	our	PRON
eurjchem-1541	136	2	com‐	com‐	ADJ
eurjchem-1541	136	3	pounds	pound	NOUN
eurjchem-1541	136	4	have	have	AUX
eurjchem-1541	136	5	showed	show	VERB
eurjchem-1541	136	6	moderateα‐amylase	moderateα‐amylase	PROPN
eurjchem-1541	136	7	and	and	CCONJ
eurjchem-1541	136	8	α‐glucosidase	α‐glucosidase	X
eurjchem-1541	136	9	inhibitory	inhibitory	ADJ
eurjchem-1541	136	10	activities	activity	NOUN
eurjchem-1541	136	11	as	as	SCONJ
eurjchem-1541	136	12	compared	compare	VERB
eurjchem-1541	136	13	to	to	ADP
eurjchem-1541	136	14	the	the	DET
eurjchem-1541	136	15	reference	reference	NOUN
eurjchem-1541	136	16	compound	compound	NOUN
eurjchem-1541	136	17	acarbose	acarbose	NOUN
eurjchem-1541	136	18	which	which	PRON
eurjchem-1541	136	19	is	be	AUX
eurjchem-1541	136	20	a	a	DET
eurjchem-1541	136	21	widely	widely	ADV
eurjchem-1541	136	22	used	use	VERB
eurjchem-1541	136	23	anti‐diabetic	anti‐diabetic	ADJ
eurjchem-1541	136	24	drug	drug	NOUN
eurjchem-1541	136	25	;	;	PUNCT
eurjchem-1541	136	26	product	product	NOUN
eurjchem-1541	136	27	f	f	PROPN
eurjchem-1541	136	28	was	be	AUX
eurjchem-1541	136	29	found	find	VERB
eurjchem-1541	136	30	most	most	ADV
eurjchem-1541	136	31	active	active	ADJ
eurjchem-1541	136	32	inhibitor	inhibitor	NOUN
eurjchem-1541	136	33	(	(	PUNCT
eurjchem-1541	136	34	ic50	ic50	PROPN
eurjchem-1541	136	35	=	=	PUNCT
eurjchem-1541	136	36	134.30	134.30	NUM
eurjchem-1541	136	37	μm	μm	NUM
eurjchem-1541	136	38	)	)	PUNCT
eurjchem-1541	136	39	for	for	ADP
eurjchem-1541	136	40	α‐	α‐	NUM
eurjchem-1541	136	41	amylase	amylase	NOUN
eurjchem-1541	136	42	,	,	PUNCT
eurjchem-1541	136	43	and	and	CCONJ
eurjchem-1541	136	44	product	product	NOUN
eurjchem-1541	136	45	b	b	PROPN
eurjchem-1541	136	46	is	be	AUX
eurjchem-1541	136	47	the	the	DET
eurjchem-1541	136	48	most	most	ADV
eurjchem-1541	136	49	active	active	ADJ
eurjchem-1541	136	50	inhibitor	inhibitor	NOUN
eurjchem-1541	136	51	(	(	PUNCT
eurjchem-1541	136	52	ic50	ic50	PROPN
eurjchem-1541	136	53	=	=	PROPN
eurjchem-1541	136	54	16.37	16.37	NUM
eurjchem-1541	136	55	μm	μm	NUM
eurjchem-1541	136	56	)	)	PUNCT
eurjchem-1541	136	57	for	for	ADP
eurjchem-1541	136	58	α‐glucosidase	α‐glucosidase	PROPN
eurjchem-1541	136	59	.	.	PUNCT
eurjchem-1541	137	1	the	the	DET
eurjchem-1541	137	2	inhibition	inhibition	NOUN
eurjchem-1541	137	3	of	of	ADP
eurjchem-1541	137	4	α‐amylase	α‐amylase	NUM
eurjchem-1541	137	5	and	and	CCONJ
eurjchem-1541	137	6	α‐glucosidase	α‐glucosidase	X
eurjchem-1541	137	7	activity	activity	NOUN
eurjchem-1541	137	8	in	in	ADP
eurjchem-1541	137	9	the	the	DET
eurjchem-1541	137	10	digestive	digestive	ADJ
eurjchem-1541	137	11	tract	tract	NOUN
eurjchem-1541	137	12	of	of	ADP
eurjchem-1541	137	13	humans	human	NOUN
eurjchem-1541	137	14	is	be	AUX
eurjchem-1541	137	15	an	an	DET
eurjchem-1541	137	16	important	important	ADJ
eurjchem-1541	137	17	strategy	strategy	NOUN
eurjchem-1541	137	18	in	in	ADP
eurjchem-1541	137	19	the	the	DET
eurjchem-1541	137	20	management	management	NOUN
eurjchem-1541	137	21	of	of	ADP
eurjchem-1541	137	22	postprandial	postprandial	ADJ
eurjchem-1541	137	23	blood	blood	NOUN
eurjchem-1541	137	24	glucose	glucose	NOUN
eurjchem-1541	137	25	level	level	NOUN
eurjchem-1541	137	26	in	in	ADP
eurjchem-1541	137	27	diabetic	diabetic	ADJ
eurjchem-1541	137	28	patients	patient	NOUN
eurjchem-1541	137	29	[	[	X
eurjchem-1541	137	30	25	25	NUM
eurjchem-1541	137	31	]	]	PUNCT
eurjchem-1541	137	32	.	.	PUNCT
eurjchem-1541	138	1	table	table	NOUN
eurjchem-1541	138	2	1	1	NUM
eurjchem-1541	138	3	.	.	PUNCT
eurjchem-1541	138	4	α‐amylase	α‐amylase	PUNCT
eurjchem-1541	138	5	and	and	CCONJ
eurjchem-1541	138	6	α‐glucosidase	α‐glucosidase	PUNCT
eurjchem-1541	138	7	inhibitory	inhibitory	ADJ
eurjchem-1541	138	8	activity	activity	NOUN
eurjchem-1541	138	9	of	of	ADP
eurjchem-1541	138	10	the	the	DET
eurjchem-1541	138	11	synthesized	synthesize	VERB
eurjchem-1541	138	12	compounds	compound	NOUN
eurjchem-1541	138	13	.	.	PUNCT
eurjchem-1541	139	1	compound	compound	NOUN
eurjchem-1541	139	2	ic50	ic50	PROPN
eurjchem-1541	139	3	(	(	PUNCT
eurjchem-1541	139	4	µm	µm	NOUN
eurjchem-1541	139	5	)	)	PUNCT
eurjchem-1541	139	6	α‐amylase	α‐amylase	PUNCT
eurjchem-1541	139	7	inhibition	inhibition	VERB
eurjchem-1541	139	8	α‐glucosidase	α‐glucosidase	NOUN
eurjchem-1541	139	9	inhibition	inhibition	NOUN
eurjchem-1541	139	10	b	b	NOUN
eurjchem-1541	139	11	347.58±0.37	347.58±0.37	NUM
eurjchem-1541	139	12	16.37±0.29	16.37±0.29	NUM
eurjchem-1541	139	13	c	c	NOUN
eurjchem-1541	139	14	1336.72±0.39	1336.72±0.39	NUM
eurjchem-1541	139	15	893.52±0.08	893.52±0.08	NUM
eurjchem-1541	140	1	d	d	NOUN
eurjchem-1541	140	2	259.40±0.17	259.40±0.17	NUM
eurjchem-1541	140	3	178.91±0.30	178.91±0.30	NUM
eurjchem-1541	140	4	e	e	NOUN
eurjchem-1541	140	5	986.25±0.41	986.25±0.41	NOUN
eurjchem-1541	140	6	690.90±0.57	690.90±0.57	NUM
eurjchem-1541	140	7	f	f	NOUN
eurjchem-1541	140	8	134.30±0.39	134.30±0.39	NUM
eurjchem-1541	140	9	89.63±0.66	89.63±0.66	NUM
eurjchem-1541	140	10	g	g	ADP
eurjchem-1541	140	11	515.80±0.37	515.80±0.37	NUM
eurjchem-1541	140	12	360.10±0.11	360.10±0.11	NUM
eurjchem-1541	140	13	acarbose	acarbose	NOUN
eurjchem-1541	140	14	482.02±1.38	482.02±1.38	NUM
eurjchem-1541	140	15	27.89±2.00	27.89±2.00	NUM
eurjchem-1541	140	16	the	the	DET
eurjchem-1541	140	17	most	most	ADV
eurjchem-1541	140	18	commonly	commonly	ADV
eurjchem-1541	140	19	used	use	VERB
eurjchem-1541	140	20	pharmacological	pharmacological	ADJ
eurjchem-1541	140	21	agents	agent	NOUN
eurjchem-1541	140	22	in	in	ADP
eurjchem-1541	140	23	the	the	DET
eurjchem-1541	140	24	treatment	treatment	NOUN
eurjchem-1541	140	25	of	of	ADP
eurjchem-1541	140	26	hyperglycemia	hyperglycemia	NOUN
eurjchem-1541	140	27	such	such	ADJ
eurjchem-1541	140	28	as	as	ADP
eurjchem-1541	140	29	acarbose	acarbose	NOUN
eurjchem-1541	140	30	is	be	AUX
eurjchem-1541	140	31	often	often	ADV
eurjchem-1541	140	32	asso‐	asso‐	AUX
eurjchem-1541	140	33	ciated	ciate	VERB
eurjchem-1541	140	34	with	with	ADP
eurjchem-1541	140	35	undesirable	undesirable	ADJ
eurjchem-1541	140	36	side	side	NOUN
eurjchem-1541	140	37	effects	effect	NOUN
eurjchem-1541	140	38	especially	especially	ADV
eurjchem-1541	140	39	abdominal	abdominal	ADJ
eurjchem-1541	140	40	distention	distention	NOUN
eurjchem-1541	140	41	,	,	PUNCT
eurjchem-1541	140	42	diarrhea	diarrhea	NOUN
eurjchem-1541	140	43	,	,	PUNCT
eurjchem-1541	140	44	and	and	CCONJ
eurjchem-1541	140	45	flatulence	flatulence	NOUN
eurjchem-1541	140	46	[	[	X
eurjchem-1541	140	47	26,27	26,27	NUM
eurjchem-1541	140	48	]	]	PUNCT
eurjchem-1541	140	49	.	.	PUNCT
eurjchem-1541	141	1	the	the	DET
eurjchem-1541	141	2	limitations	limitation	NOUN
eurjchem-1541	141	3	of	of	ADP
eurjchem-1541	141	4	currently	currently	ADV
eurjchem-1541	141	5	available	available	ADJ
eurjchem-1541	141	6	drugs	drug	NOUN
eurjchem-1541	141	7	for	for	ADP
eurjchem-1541	141	8	the	the	DET
eurjchem-1541	141	9	control	control	NOUN
eurjchem-1541	141	10	of	of	ADP
eurjchem-1541	141	11	blood	blood	NOUN
eurjchem-1541	141	12	glucose	glucose	NOUN
eurjchem-1541	141	13	have	have	AUX
eurjchem-1541	141	14	stimulated	stimulate	VERB
eurjchem-1541	141	15	research	research	NOUN
eurjchem-1541	141	16	on	on	ADP
eurjchem-1541	141	17	novel	novel	ADJ
eurjchem-1541	141	18	anti‐hyperglecemic	anti‐hyperglecemic	ADJ
eurjchem-1541	141	19	drugs	drug	NOUN
eurjchem-1541	141	20	.	.	PUNCT
eurjchem-1541	142	1	the	the	DET
eurjchem-1541	142	2	results	result	NOUN
eurjchem-1541	142	3	of	of	ADP
eurjchem-1541	142	4	our	our	PRON
eurjchem-1541	142	5	study	study	NOUN
eurjchem-1541	142	6	may	may	AUX
eurjchem-1541	142	7	suggest	suggest	VERB
eurjchem-1541	142	8	these	these	DET
eurjchem-1541	142	9	synthetic	synthetic	ADJ
eurjchem-1541	142	10	compounds	compound	NOUN
eurjchem-1541	142	11	as	as	ADP
eurjchem-1541	142	12	new	new	ADJ
eurjchem-1541	142	13	molecular	molecular	ADJ
eurjchem-1541	142	14	templates	template	NOUN
eurjchem-1541	142	15	for	for	ADP
eurjchem-1541	142	16	development	development	NOUN
eurjchem-1541	142	17	of	of	ADP
eurjchem-1541	142	18	novel	novel	ADJ
eurjchem-1541	142	19	agents	agent	NOUN
eurjchem-1541	142	20	for	for	ADP
eurjchem-1541	142	21	the	the	DET
eurjchem-1541	142	22	management	management	NOUN
eurjchem-1541	142	23	of	of	ADP
eurjchem-1541	142	24	postprandial	postprandial	ADJ
eurjchem-1541	142	25	hyperglycemia	hyperglycemia	NOUN
eurjchem-1541	142	26	.	.	PUNCT
eurjchem-1541	143	1	4	4	X
eurjchem-1541	143	2	.	.	X
eurjchem-1541	143	3	conclusion	conclusion	NOUN
eurjchem-1541	143	4	in	in	ADP
eurjchem-1541	143	5	conclusion	conclusion	NOUN
eurjchem-1541	143	6	,	,	PUNCT
eurjchem-1541	143	7	a	a	DET
eurjchem-1541	143	8	series	series	NOUN
eurjchem-1541	143	9	of	of	ADP
eurjchem-1541	143	10	pyrazolo[3,4‐d]pyrimidine	pyrazolo[3,4‐d]pyrimidine	NOUN
eurjchem-1541	143	11	deri‐	deri‐	DET
eurjchem-1541	143	12	vatives	vative	NOUN
eurjchem-1541	143	13	were	be	AUX
eurjchem-1541	143	14	synthesized	synthesize	VERB
eurjchem-1541	143	15	successfully	successfully	ADV
eurjchem-1541	143	16	via	via	ADP
eurjchem-1541	143	17	thionation	thionation	NOUN
eurjchem-1541	143	18	,	,	PUNCT
eurjchem-1541	143	19	alky‐	alky‐	PUNCT
eurjchem-1541	143	20	lation	lation	NOUN
eurjchem-1541	143	21	and	and	CCONJ
eurjchem-1541	143	22	1,3‐dipolar	1,3‐dipolar	NUM
eurjchem-1541	143	23	cycloaddition	cycloaddition	NOUN
eurjchem-1541	143	24	reactions	reaction	NOUN
eurjchem-1541	143	25	and	and	CCONJ
eurjchem-1541	143	26	cyclization	cyclization	NOUN
eurjchem-1541	143	27	.	.	PUNCT
eurjchem-1541	144	1	all	all	DET
eurjchem-1541	144	2	these	these	DET
eurjchem-1541	144	3	new	new	ADJ
eurjchem-1541	144	4	compounds	compound	NOUN
eurjchem-1541	144	5	were	be	AUX
eurjchem-1541	144	6	confirmed	confirm	VERB
eurjchem-1541	144	7	by	by	ADP
eurjchem-1541	144	8	ms	ms	PROPN
eurjchem-1541	144	9	,	,	PUNCT
eurjchem-1541	144	10	ft‐ir	ft‐ir	NOUN
eurjchem-1541	144	11	and	and	CCONJ
eurjchem-1541	144	12	nmr	nmr	NOUN
eurjchem-1541	144	13	spectral	spectral	ADJ
eurjchem-1541	144	14	techniques	technique	NOUN
eurjchem-1541	144	15	.	.	PUNCT
eurjchem-1541	145	1	their	their	PRON
eurjchem-1541	145	2	α‐amylase	α‐amylase	NUM
eurjchem-1541	145	3	and	and	CCONJ
eurjchem-1541	145	4	α‐glucosidase	α‐glucosidase	X
eurjchem-1541	145	5	inhibitory	inhibitory	ADJ
eurjchem-1541	145	6	activities	activity	NOUN
eurjchem-1541	145	7	were	be	AUX
eurjchem-1541	145	8	evaluated	evaluate	VERB
eurjchem-1541	145	9	.	.	PUNCT
eurjchem-1541	146	1	the	the	DET
eurjchem-1541	146	2	results	result	NOUN
eurjchem-1541	146	3	showed	show	VERB
eurjchem-1541	146	4	that	that	SCONJ
eurjchem-1541	146	5	most	most	ADJ
eurjchem-1541	146	6	of	of	ADP
eurjchem-1541	146	7	the	the	DET
eurjchem-1541	146	8	synthesized	synthesize	VERB
eurjchem-1541	146	9	pyrazolo[3,4‐d]pyrimidine	pyrazolo[3,4‐d]pyrimidine	NOUN
eurjchem-1541	146	10	derivatives	derivative	NOUN
eurjchem-1541	146	11	exhibited	exhibit	VERB
eurjchem-1541	146	12	moderate	moderate	ADJ
eurjchem-1541	146	13	inhibition	inhibition	NOUN
eurjchem-1541	146	14	of	of	ADP
eurjchem-1541	146	15	α‐amylase	α‐amylase	NUM
eurjchem-1541	146	16	and	and	CCONJ
eurjchem-1541	146	17	α‐glucosidase	α‐glucosidase	PUNCT
eurjchem-1541	146	18	activities	activity	NOUN
eurjchem-1541	146	19	,	,	PUNCT
eurjchem-1541	146	20	product	product	NOUN
eurjchem-1541	146	21	f	f	PROPN
eurjchem-1541	146	22	was	be	AUX
eurjchem-1541	146	23	found	find	VERB
eurjchem-1541	146	24	most	most	ADV
eurjchem-1541	146	25	active	active	ADJ
eurjchem-1541	146	26	inhibitor	inhibitor	NOUN
eurjchem-1541	146	27	(	(	PUNCT
eurjchem-1541	146	28	ic50	ic50	PROPN
eurjchem-1541	146	29	=	=	PUNCT
eurjchem-1541	146	30	134.30	134.30	NUM
eurjchem-1541	146	31	μm	μm	NOUN
eurjchem-1541	146	32	)	)	PUNCT
eurjchem-1541	146	33	for	for	ADP
eurjchem-1541	146	34	α‐amylase	α‐amylase	NUM
eurjchem-1541	146	35	,	,	PUNCT
eurjchem-1541	146	36	and	and	CCONJ
eurjchem-1541	146	37	product	product	NOUN
eurjchem-1541	146	38	b	b	PROPN
eurjchem-1541	146	39	is	be	AUX
eurjchem-1541	146	40	the	the	DET
eurjchem-1541	146	41	most	most	ADV
eurjchem-1541	146	42	active	active	ADJ
eurjchem-1541	146	43	inhibitor	inhibitor	NOUN
eurjchem-1541	146	44	(	(	PUNCT
eurjchem-1541	146	45	ic50	ic50	PROPN
eurjchem-1541	146	46	=	=	PROPN
eurjchem-1541	146	47	16.37	16.37	NUM
eurjchem-1541	146	48	μm	μm	NUM
eurjchem-1541	146	49	)	)	PUNCT
eurjchem-1541	146	50	for	for	ADP
eurjchem-1541	146	51	α‐glucosidase	α‐glucosidase	PROPN
eurjchem-1541	146	52	.	.	PROPN
eurjchem-1541	146	53	acknowledgement	acknowledgement	NOUN
eurjchem-1541	146	54	the	the	DET
eurjchem-1541	146	55	authors	author	NOUN
eurjchem-1541	146	56	thank	thank	VERB
eurjchem-1541	146	57	pharmaceutical	pharmaceutical	NOUN
eurjchem-1541	146	58	laboratories	laboratory	NOUN
eurjchem-1541	146	59	sothema	sothema	VERB
eurjchem-1541	146	60	for	for	ADP
eurjchem-1541	146	61	supporting	support	VERB
eurjchem-1541	146	62	this	this	DET
eurjchem-1541	146	63	study	study	NOUN
eurjchem-1541	146	64	(	(	PUNCT
eurjchem-1541	146	65	for	for	ADP
eurjchem-1541	146	66	disposal	disposal	NOUN
eurjchem-1541	146	67	of	of	ADP
eurjchem-1541	146	68	the	the	DET
eurjchem-1541	146	69	raw	raw	ADJ
eurjchem-1541	146	70	material	material	NOUN
eurjchem-1541	146	71	,	,	PUNCT
eurjchem-1541	146	72	allopurinol	allopurinol	NOUN
eurjchem-1541	146	73	)	)	PUNCT
eurjchem-1541	146	74	.	.	PUNCT
eurjchem-1541	147	1	references	reference	NOUN
eurjchem-1541	147	2	[	[	X
eurjchem-1541	147	3	1	1	NUM
eurjchem-1541	147	4	]	]	PUNCT
eurjchem-1541	147	5	.	.	PUNCT
eurjchem-1541	148	1	idf	idf	PROPN
eurjchem-1541	148	2	diabetes	diabetes	PROPN
eurjchem-1541	148	3	atlas	atlas	PROPN
eurjchem-1541	148	4	.	.	PUNCT
eurjchem-1541	148	5	brussels	brussels	PROPN
eurjchem-1541	148	6	,	,	PUNCT
eurjchem-1541	148	7	belgium	belgium	PROPN
eurjchem-1541	148	8	:	:	PUNCT
eurjchem-1541	148	9	international	international	ADJ
eurjchem-1541	148	10	diabetes	diabetes	PROPN
eurjchem-1541	148	11	federation	federation	NOUN
eurjchem-1541	148	12	,	,	PUNCT
eurjchem-1541	148	13	7th	7th	ADJ
eurjchem-1541	148	14	ed	ed	NOUN
eurjchem-1541	148	15	.	.	PROPN
eurjchem-1541	148	16	2015	2015	NUM
eurjchem-1541	148	17	,	,	PUNCT
eurjchem-1541	148	18	http://www.diabetesatlas.org	http://www.diabetesatlas.org	X
eurjchem-1541	149	1	[	[	X
eurjchem-1541	149	2	2	2	NUM
eurjchem-1541	149	3	]	]	PUNCT
eurjchem-1541	149	4	.	.	PUNCT
eurjchem-1541	150	1	rossi	rossi	PROPN
eurjchem-1541	150	2	,	,	PUNCT
eurjchem-1541	150	3	e.	e.	PROPN
eurjchem-1541	150	4	j.	j.	PROPN
eurjchem-1541	150	5	;	;	PUNCT
eurjchem-1541	150	6	sim	sim	PROPN
eurjchem-1541	150	7	,	,	PUNCT
eurjchem-1541	150	8	l.	l.	PROPN
eurjchem-1541	150	9	;	;	PUNCT
eurjchem-1541	150	10	kuntz	kuntz	PROPN
eurjchem-1541	150	11	,	,	PUNCT
eurjchem-1541	150	12	d.	d.	PROPN
eurjchem-1541	150	13	a.	a.	PROPN
eurjchem-1541	150	14	;	;	PUNCT
eurjchem-1541	150	15	hahn	hahn	PROPN
eurjchem-1541	150	16	,	,	PUNCT
eurjchem-1541	150	17	d.	d.	PROPN
eurjchem-1541	150	18	;	;	PUNCT
eurjchem-1541	150	19	johnston	johnston	PROPN
eurjchem-1541	150	20	,	,	PUNCT
eurjchem-1541	150	21	b.	b.	PROPN
eurjchem-1541	150	22	d.	d.	PROPN
eurjchem-1541	150	23	;	;	PUNCT
eurjchem-1541	150	24	ghavami	ghavami	NOUN
eurjchem-1541	150	25	,	,	PUNCT
eurjchem-1541	150	26	a.	a.	NOUN
eurjchem-1541	150	27	;	;	PUNCT
eurjchem-1541	150	28	rose	rise	VERB
eurjchem-1541	150	29	,	,	PUNCT
eurjchem-1541	150	30	d.	d.	PROPN
eurjchem-1541	150	31	r.	r.	PROPN
eurjchem-1541	150	32	fed	fed	PROPN
eurjchem-1541	150	33	.	.	PUNCT
eurjchem-1541	151	1	eur	eur	PROPN
eurjchem-1541	151	2	.	.	PUNCT
eurjchem-1541	152	1	biochem	biochem	PROPN
eurjchem-1541	152	2	.	.	PUNCT
eurjchem-1541	153	1	soc	soc	PROPN
eurjchem-1541	153	2	.	.	PUNCT
eurjchem-1541	154	1	j.	j.	PROPN
eurjchem-1541	154	2	2006	2006	NUM
eurjchem-1541	154	3	,	,	PUNCT
eurjchem-1541	154	4	273	273	NUM
eurjchem-1541	154	5	,	,	PUNCT
eurjchem-1541	154	6	2673‐2683	2673‐2683	NUM
eurjchem-1541	154	7	.	.	PUNCT
eurjchem-1541	155	1	[	[	X
eurjchem-1541	155	2	3	3	NUM
eurjchem-1541	155	3	]	]	PUNCT
eurjchem-1541	155	4	.	.	PUNCT
eurjchem-1541	156	1	matthews	matthews	PROPN
eurjchem-1541	156	2	,	,	PUNCT
eurjchem-1541	156	3	d.	d.	PROPN
eurjchem-1541	156	4	r.	r.	PROPN
eurjchem-1541	156	5	;	;	PUNCT
eurjchem-1541	156	6	hosker	hosker	PROPN
eurjchem-1541	156	7	,	,	PUNCT
eurjchem-1541	156	8	j.	j.	PROPN
eurjchem-1541	156	9	p.	p.	PROPN
eurjchem-1541	156	10	;	;	PUNCT
eurjchem-1541	156	11	rudenski	rudenski	NOUN
eurjchem-1541	156	12	,	,	PUNCT
eurjchem-1541	156	13	a.	a.	PROPN
eurjchem-1541	156	14	s.	s.	PROPN
eurjchem-1541	156	15	;	;	PUNCT
eurjchem-1541	156	16	naylor	naylor	PROPN
eurjchem-1541	156	17	,	,	PUNCT
eurjchem-1541	156	18	b.	b.	PROPN
eurjchem-1541	156	19	a.	a.	PROPN
eurjchem-1541	156	20	;	;	PUNCT
eurjchem-1541	156	21	treacher	treacher	PROPN
eurjchem-1541	156	22	,	,	PUNCT
eurjchem-1541	156	23	d.	d.	PROPN
eurjchem-1541	156	24	f.	f.	PROPN
eurjchem-1541	156	25	;	;	PUNCT
eurjchem-1541	156	26	turner	turner	PROPN
eurjchem-1541	156	27	,	,	PUNCT
eurjchem-1541	156	28	r.	r.	PROPN
eurjchem-1541	156	29	c.	c.	PROPN
eurjchem-1541	156	30	diabetologia	diabetologia	PROPN
eurjchem-1541	156	31	.	.	PUNCT
eurjchem-1541	157	1	1985	1985	NUM
eurjchem-1541	157	2	,	,	PUNCT
eurjchem-1541	157	3	28	28	NUM
eurjchem-1541	157	4	,	,	PUNCT
eurjchem-1541	157	5	412‐419	412‐419	NUM
eurjchem-1541	157	6	.	.	PUNCT
eurjchem-1541	158	1	[	[	X
eurjchem-1541	158	2	4	4	NUM
eurjchem-1541	158	3	]	]	PUNCT
eurjchem-1541	158	4	.	.	PUNCT
eurjchem-1541	159	1	kawahito	kawahito	PROPN
eurjchem-1541	159	2	,	,	PUNCT
eurjchem-1541	159	3	s.	s.	PROPN
eurjchem-1541	159	4	;	;	PUNCT
eurjchem-1541	159	5	kitahata	kitahata	PROPN
eurjchem-1541	159	6	,	,	PUNCT
eurjchem-1541	159	7	h.	h.	PROPN
eurjchem-1541	159	8	;	;	PUNCT
eurjchem-1541	159	9	oshita	oshita	PROPN
eurjchem-1541	159	10	,	,	PUNCT
eurjchem-1541	159	11	s.	s.	PROPN
eurjchem-1541	159	12	world	world	PROPN
eurjchem-1541	159	13	j.	j.	PROPN
eurjchem-1541	159	14	gastroentero	gastroentero	PROPN
eurjchem-1541	159	15	.	.	PUNCT
eurjchem-1541	160	1	2009	2009	NUM
eurjchem-1541	160	2	,	,	PUNCT
eurjchem-1541	160	3	15	15	NUM
eurjchem-1541	160	4	,	,	PUNCT
eurjchem-1541	160	5	4137‐4142	4137‐4142	NUM
eurjchem-1541	160	6	.	.	PUNCT
eurjchem-1541	161	1	[	[	X
eurjchem-1541	161	2	5	5	NUM
eurjchem-1541	161	3	]	]	PUNCT
eurjchem-1541	161	4	.	.	PUNCT
eurjchem-1541	161	5	saltos	salto	NOUN
eurjchem-1541	161	6	,	,	PUNCT
eurjchem-1541	161	7	m.	m.	PROPN
eurjchem-1541	161	8	b.	b.	PROPN
eurjchem-1541	162	1	v.	v.	PROPN
eurjchem-1541	162	2	;	;	PUNCT
eurjchem-1541	162	3	puente	puente	PROPN
eurjchem-1541	162	4	,	,	PUNCT
eurjchem-1541	162	5	b.	b.	PROPN
eurjchem-1541	162	6	f.	f.	PROPN
eurjchem-1541	162	7	n.	n.	PROPN
eurjchem-1541	162	8	;	;	PUNCT
eurjchem-1541	162	9	faraone	faraone	NOUN
eurjchem-1541	162	10	,	,	PUNCT
eurjchem-1541	162	11	i.	i.	NOUN
eurjchem-1541	162	12	;	;	PUNCT
eurjchem-1541	162	13	milella	milella	PROPN
eurjchem-1541	162	14	,	,	PUNCT
eurjchem-1541	162	15	l.	l.	PROPN
eurjchem-1541	162	16	;	;	PUNCT
eurjchem-1541	162	17	de	de	X
eurjchem-1541	162	18	tommasi	tommasi	PROPN
eurjchem-1541	162	19	,	,	PUNCT
eurjchem-1541	162	20	n.	n.	NOUN
eurjchem-1541	162	21	;	;	PUNCT
eurjchem-1541	162	22	braca	braca	PROPN
eurjchem-1541	162	23	,	,	PUNCT
eurjchem-1541	162	24	a.	a.	PROPN
eurjchem-1541	162	25	phytochem	phytochem	PROPN
eurjchem-1541	162	26	.	.	PUNCT
eurjchem-1541	163	1	lett	lett	PROPN
eurjchem-1541	163	2	.	.	PROPN
eurjchem-1541	164	1	2015	2015	NUM
eurjchem-1541	164	2	,	,	PUNCT
eurjchem-1541	164	3	14	14	NUM
eurjchem-1541	164	4	,	,	PUNCT
eurjchem-1541	164	5	45‐50	45‐50	NUM
eurjchem-1541	164	6	.	.	PUNCT
eurjchem-1541	165	1	[	[	X
eurjchem-1541	165	2	6	6	NUM
eurjchem-1541	165	3	]	]	PUNCT
eurjchem-1541	165	4	.	.	PUNCT
eurjchem-1541	166	1	kim	kim	PROPN
eurjchem-1541	166	2	,	,	PUNCT
eurjchem-1541	166	3	j.	j.	PROPN
eurjchem-1541	166	4	s.	s.	PROPN
eurjchem-1541	166	5	;	;	PUNCT
eurjchem-1541	166	6	kwon	kwon	PROPN
eurjchem-1541	166	7	,	,	PUNCT
eurjchem-1541	166	8	c.	c.	PROPN
eurjchem-1541	166	9	s.	s.	PROPN
eurjchem-1541	166	10	;	;	PUNCT
eurjchem-1541	166	11	son	son	PROPN
eurjchem-1541	166	12	,	,	PUNCT
eurjchem-1541	166	13	k.	k.	PROPN
eurjchem-1541	166	14	h.	h.	PROPN
eurjchem-1541	166	15	biosci	biosci	PROPN
eurjchem-1541	166	16	.	.	PUNCT
eurjchem-1541	167	1	biotech	biotech	PROPN
eurjchem-1541	167	2	.	.	PUNCT
eurjchem-1541	168	1	bioch	bioch	PROPN
eurjchem-1541	168	2	.	.	PUNCT
eurjchem-1541	169	1	2000	2000	NUM
eurjchem-1541	169	2	,	,	PUNCT
eurjchem-1541	169	3	64	64	NUM
eurjchem-1541	169	4	,	,	PUNCT
eurjchem-1541	169	5	2458‐	2458‐	NUM
eurjchem-1541	169	6	2461	2461	NUM
eurjchem-1541	169	7	.	.	PUNCT
eurjchem-1541	170	1	[	[	X
eurjchem-1541	170	2	7	7	NUM
eurjchem-1541	170	3	]	]	PUNCT
eurjchem-1541	170	4	.	.	PUNCT
eurjchem-1541	171	1	kwon	kwon	PROPN
eurjchem-1541	171	2	,	,	PUNCT
eurjchem-1541	171	3	y.	y.	PROPN
eurjchem-1541	171	4	i.	i.	PROPN
eurjchem-1541	171	5	;	;	PUNCT
eurjchem-1541	171	6	apostolidis	apostolidis	PROPN
eurjchem-1541	171	7	,	,	PUNCT
eurjchem-1541	171	8	e.	e.	PROPN
eurjchem-1541	171	9	;	;	PUNCT
eurjchem-1541	171	10	shetty	shetty	PROPN
eurjchem-1541	171	11	,	,	PUNCT
eurjchem-1541	171	12	k.	k.	PROPN
eurjchem-1541	171	13	j.	j.	PROPN
eurjchem-1541	171	14	food	food	PROPN
eurjchem-1541	171	15	biochem	biochem	PROPN
eurjchem-1541	171	16	.	.	PUNCT
eurjchem-1541	172	1	2007	2007	NUM
eurjchem-1541	172	2	,	,	PUNCT
eurjchem-1541	172	3	31	31	NUM
eurjchem-1541	172	4	,	,	PUNCT
eurjchem-1541	172	5	370‐	370‐	NUM
eurjchem-1541	172	6	385	385	NUM
eurjchem-1541	172	7	.	.	PUNCT
eurjchem-1541	173	1	[	[	X
eurjchem-1541	173	2	8	8	NUM
eurjchem-1541	173	3	]	]	PUNCT
eurjchem-1541	173	4	.	.	PUNCT
eurjchem-1541	174	1	hano	hano	PROPN
eurjchem-1541	174	2	,	,	PUNCT
eurjchem-1541	174	3	c.	c.	PROPN
eurjchem-1541	174	4	;	;	PUNCT
eurjchem-1541	174	5	renouard	renouard	ADV
eurjchem-1541	174	6	,	,	PUNCT
eurjchem-1541	174	7	s.	s.	PROPN
eurjchem-1541	174	8	;	;	PUNCT
eurjchem-1541	174	9	molinie	molinie	PROPN
eurjchem-1541	174	10	,	,	PUNCT
eurjchem-1541	174	11	r.	r.	PROPN
eurjchem-1541	174	12	bioorg	bioorg	PROPN
eurjchem-1541	174	13	.	.	PUNCT
eurjchem-1541	175	1	med	med	PROPN
eurjchem-1541	175	2	.	.	PROPN
eurjchem-1541	175	3	chem	chem	PROPN
eurjchem-1541	175	4	.	.	PUNCT
eurjchem-1541	176	1	lett	lett	PROPN
eurjchem-1541	176	2	.	.	PUNCT
eurjchem-1541	177	1	2013	2013	NUM
eurjchem-1541	177	2	,	,	PUNCT
eurjchem-1541	177	3	23	23	NUM
eurjchem-1541	177	4	,	,	PUNCT
eurjchem-1541	177	5	3007‐3012	3007‐3012	NUM
eurjchem-1541	177	6	.	.	PUNCT
eurjchem-1541	178	1	[	[	X
eurjchem-1541	178	2	9	9	NUM
eurjchem-1541	178	3	]	]	PUNCT
eurjchem-1541	178	4	.	.	PUNCT
eurjchem-1541	178	5	ramadhan	ramadhan	PROPN
eurjchem-1541	178	6	,	,	PUNCT
eurjchem-1541	178	7	r.	r.	PROPN
eurjchem-1541	178	8	;	;	PUNCT
eurjchem-1541	178	9	phuwapraisirisan	phuwapraisirisan	PROPN
eurjchem-1541	178	10	,	,	PUNCT
eurjchem-1541	178	11	p.	p.	PROPN
eurjchem-1541	178	12	bioorg	bioorg	PROPN
eurjchem-1541	178	13	.	.	PUNCT
eurjchem-1541	179	1	med	med	PROPN
eurjchem-1541	179	2	.	.	PROPN
eurjchem-1541	179	3	chem	chem	PROPN
eurjchem-1541	179	4	.	.	PUNCT
eurjchem-1541	180	1	lett	lett	PROPN
eurjchem-1541	180	2	.	.	PROPN
eurjchem-1541	181	1	2015	2015	NUM
eurjchem-1541	181	2	,	,	PUNCT
eurjchem-1541	181	3	25	25	NUM
eurjchem-1541	181	4	,	,	PUNCT
eurjchem-1541	181	5	2529‐2533	2529‐2533	NUM
eurjchem-1541	181	6	.	.	PUNCT
eurjchem-1541	182	1	[	[	X
eurjchem-1541	182	2	10	10	NUM
eurjchem-1541	182	3	]	]	PUNCT
eurjchem-1541	182	4	.	.	PUNCT
eurjchem-1541	183	1	mahmoud	mahmoud	PROPN
eurjchem-1541	183	2	,	,	PUNCT
eurjchem-1541	183	3	h.	h.	PROPN
eurjchem-1541	183	4	i.	i.	PROPN
eurjchem-1541	183	5	;	;	PUNCT
eurjchem-1541	183	6	el‐rab	el‐rab	PROPN
eurjchem-1541	183	7	,	,	PUNCT
eurjchem-1541	183	8	s.	s.	PROPN
eurjchem-1541	183	9	m.	m.	PROPN
eurjchem-1541	183	10	g.	g.	PROPN
eurjchem-1541	183	11	b	b	PROPN
eurjchem-1541	183	12	,	,	PUNCT
eurjchem-1541	183	13	khalil	khalil	PROPN
eurjchem-1541	183	14	,	,	PUNCT
eurjchem-1541	183	15	a.	a.	PROPN
eurjchem-1541	183	16	f.	f.	PROPN
eurjchem-1541	183	17	;	;	PUNCT
eurjchem-1541	183	18	ismael	ismael	PROPN
eurjchem-1541	183	19	,	,	PUNCT
eurjchem-1541	183	20	s.	s.	PROPN
eurjchem-1541	183	21	m.	m.	PROPN
eurjchem-1541	183	22	eur	eur	PROPN
eurjchem-1541	183	23	.	.	PUNCT
eurjchem-1541	184	1	j.	j.	PROPN
eurjchem-1541	184	2	chem	chem	PROPN
eurjchem-1541	184	3	.	.	PUNCT
eurjchem-1541	185	1	2014	2014	NUM
eurjchem-1541	185	2	,	,	PUNCT
eurjchem-1541	185	3	5	5	NUM
eurjchem-1541	185	4	,	,	PUNCT
eurjchem-1541	185	5	65‐72	65‐72	NUM
eurjchem-1541	185	6	.	.	PUNCT
eurjchem-1541	186	1	[	[	X
eurjchem-1541	186	2	11	11	NUM
eurjchem-1541	186	3	]	]	PUNCT
eurjchem-1541	186	4	.	.	PUNCT
eurjchem-1541	187	1	taher	taher	PROPN
eurjchem-1541	187	2	,	,	PUNCT
eurjchem-1541	187	3	m.	m.	PROPN
eurjchem-1541	187	4	a.	a.	PROPN
eurjchem-1541	187	5	h.	h.	PROPN
eurjchem-1541	187	6	;	;	PUNCT
eurjchem-1541	187	7	dawood	dawood	PROPN
eurjchem-1541	187	8	,	,	PUNCT
eurjchem-1541	187	9	d.	d.	PROPN
eurjchem-1541	187	10	h.	h.	PROPN
eurjchem-1541	187	11	;	;	PUNCT
eurjchem-1541	187	12	sanad	sanad	NOUN
eurjchem-1541	187	13	,	,	PUNCT
eurjchem-1541	187	14	m.	m.	NOUN
eurjchem-1541	187	15	i.	i.	PROPN
eurjchem-1541	187	16	;	;	PUNCT
eurjchem-1541	187	17	hassan	hassan	PROPN
eurjchem-1541	187	18	,	,	PUNCT
eurjchem-1541	187	19	r.	r.	PROPN
eurjchem-1541	187	20	a.	a.	PROPN
eurjchem-1541	187	21	eur	eur	PROPN
eurjchem-1541	187	22	.	.	PUNCT
eurjchem-1541	188	1	j.	j.	PROPN
eurjchem-1541	188	2	chem	chem	PROPN
eurjchem-1541	188	3	.	.	PUNCT
eurjchem-1541	189	1	2016	2016	NUM
eurjchem-1541	189	2	,	,	PUNCT
eurjchem-1541	189	3	7	7	NUM
eurjchem-1541	189	4	,	,	PUNCT
eurjchem-1541	189	5	397‐404	397‐404	NOUN
eurjchem-1541	189	6	.	.	PUNCT
eurjchem-1541	190	1	[	[	X
eurjchem-1541	190	2	12	12	NUM
eurjchem-1541	190	3	]	]	PUNCT
eurjchem-1541	190	4	.	.	PUNCT
eurjchem-1541	191	1	mcinnes	mcinne	NOUN
eurjchem-1541	191	2	,	,	PUNCT
eurjchem-1541	191	3	g.	g.	PROPN
eurjchem-1541	191	4	t.	t.	PROPN
eurjchem-1541	191	5	;	;	PUNCT
eurjchem-1541	191	6	lawson	lawson	PROPN
eurjchem-1541	191	7	,	,	PUNCT
eurjchem-1541	191	8	d.	d.	PROPN
eurjchem-1541	191	9	h.	h.	PROPN
eurjchem-1541	191	10	;	;	PUNCT
eurjchem-1541	191	11	jick	jick	PROPN
eurjchem-1541	191	12	,	,	PUNCT
eurjchem-1541	191	13	h.	h.	PROPN
eurjchem-1541	191	14	ann	ann	PROPN
eurjchem-1541	191	15	.	.	PUNCT
eurjchem-1541	192	1	rheum	rheum	PROPN
eurjchem-1541	192	2	.	.	PUNCT
eurjchem-1541	193	1	dis	dis	PROPN
eurjchem-1541	193	2	.	.	PUNCT
eurjchem-1541	194	1	1981	1981	NUM
eurjchem-1541	194	2	,	,	PUNCT
eurjchem-1541	194	3	40	40	NUM
eurjchem-1541	194	4	,	,	PUNCT
eurjchem-1541	194	5	245‐	245‐	NUM
eurjchem-1541	194	6	249	249	NUM
eurjchem-1541	194	7	.	.	PUNCT
eurjchem-1541	195	1	[	[	X
eurjchem-1541	195	2	13	13	NUM
eurjchem-1541	195	3	]	]	PUNCT
eurjchem-1541	195	4	.	.	PUNCT
eurjchem-1541	196	1	gruchalla	gruchalla	PROPN
eurjchem-1541	196	2	,	,	PUNCT
eurjchem-1541	196	3	r.	r.	PROPN
eurjchem-1541	196	4	s.	s.	PROPN
eurjchem-1541	196	5	;	;	PUNCT
eurjchem-1541	196	6	j.	j.	PROPN
eurjchem-1541	196	7	allergy	allergy	PROPN
eurjchem-1541	196	8	clin	clin	PROPN
eurjchem-1541	196	9	.	.	PUNCT
eurjchem-1541	197	1	immunol	immunol	PROPN
eurjchem-1541	197	2	.	.	PUNCT
eurjchem-1541	198	1	2003	2003	NUM
eurjchem-1541	198	2	,	,	PUNCT
eurjchem-1541	198	3	111	111	NUM
eurjchem-1541	198	4	,	,	PUNCT
eurjchem-1541	198	5	548‐559	548‐559	NUM
eurjchem-1541	198	6	.	.	PUNCT
eurjchem-1541	199	1	[	[	X
eurjchem-1541	199	2	14	14	NUM
eurjchem-1541	199	3	]	]	PUNCT
eurjchem-1541	199	4	.	.	PUNCT
eurjchem-1541	199	5	zimmerman	zimmerman	PROPN
eurjchem-1541	199	6	,	,	PUNCT
eurjchem-1541	199	7	h.	h.	PROPN
eurjchem-1541	199	8	j.	j.	PROPN
eurjchem-1541	199	9	;	;	PUNCT
eurjchem-1541	199	10	maddrey	maddrey	PROPN
eurjchem-1541	199	11	,	,	PUNCT
eurjchem-1541	199	12	w.	w.	PROPN
eurjchem-1541	199	13	c.	c.	PROPN
eurjchem-1541	199	14	hepatology	hepatology	PROPN
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eurjchem-1541	199	16	,	,	PUNCT
eurjchem-1541	199	17	22	22	NUM
eurjchem-1541	199	18	,	,	PUNCT
eurjchem-1541	199	19	767‐773	767‐773	NUM
eurjchem-1541	199	20	.	.	PUNCT
eurjchem-1541	200	1	[	[	X
eurjchem-1541	200	2	15	15	NUM
eurjchem-1541	200	3	]	]	PUNCT
eurjchem-1541	200	4	.	.	PUNCT
eurjchem-1541	201	1	horsmans	horsman	NOUN
eurjchem-1541	201	2	,	,	PUNCT
eurjchem-1541	201	3	y.	y.	PROPN
eurjchem-1541	201	4	gastroenterol	gastroenterol	PROPN
eurjchem-1541	201	5	clin	clin	PROPN
eurjchem-1541	201	6	.	.	PUNCT
eurjchem-1541	202	1	biol	biol	PROPN
eurjchem-1541	202	2	.	.	PUNCT
eurjchem-1541	203	1	1993	1993	NUM
eurjchem-1541	203	2	,	,	PUNCT
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eurjchem-1541	203	4	,	,	PUNCT
eurjchem-1541	203	5	25‐30	25‐30	NOUN
eurjchem-1541	203	6	.	.	PUNCT
eurjchem-1541	204	1	[	[	X
eurjchem-1541	204	2	16	16	NUM
eurjchem-1541	204	3	]	]	PUNCT
eurjchem-1541	204	4	.	.	PUNCT
eurjchem-1541	205	1	el	el	PROPN
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eurjchem-1541	205	3	,	,	PUNCT
eurjchem-1541	205	4	m.	m.	NOUN
eurjchem-1541	205	5	;	;	PUNCT
eurjchem-1541	205	6	ramli	ramli	PROPN
eurjchem-1541	205	7	,	,	PUNCT
eurjchem-1541	205	8	y.	y.	PROPN
eurjchem-1541	205	9	;	;	PUNCT
eurjchem-1541	205	10	essassi	essassi	PROPN
eurjchem-1541	205	11	,	,	PUNCT
eurjchem-1541	205	12	e.	e.	PROPN
eurjchem-1541	205	13	m.	m.	PROPN
eurjchem-1541	205	14	;	;	PUNCT
eurjchem-1541	205	15	saadi	saadi	NOUN
eurjchem-1541	205	16	,	,	PUNCT
eurjchem-1541	205	17	m.	m.	NOUN
eurjchem-1541	205	18	;	;	PUNCT
eurjchem-1541	205	19	el	el	PROPN
eurjchem-1541	205	20	ammari	ammari	PROPN
eurjchem-1541	205	21	,	,	PUNCT
eurjchem-1541	205	22	l.	l.	PROPN
eurjchem-1541	205	23	acta	acta	PROPN
eurjchem-1541	205	24	cryst	cryst	PROPN
eurjchem-1541	205	25	.	.	PUNCT
eurjchem-1541	206	1	e	e	PROPN
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eurjchem-1541	206	3	,	,	PUNCT
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eurjchem-1541	206	5	,	,	PUNCT
eurjchem-1541	206	6	o1005‐o1006	o1005‐o1006	NOUN
eurjchem-1541	206	7	.	.	PUNCT
eurjchem-1541	207	1	[	[	X
eurjchem-1541	207	2	17	17	NUM
eurjchem-1541	207	3	]	]	PUNCT
eurjchem-1541	207	4	.	.	PUNCT
eurjchem-1541	208	1	el	el	PROPN
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eurjchem-1541	208	3	,	,	PUNCT
eurjchem-1541	208	4	m.	m.	NOUN
eurjchem-1541	208	5	;	;	PUNCT
eurjchem-1541	208	6	ramli	ramli	PROPN
eurjchem-1541	208	7	,	,	PUNCT
eurjchem-1541	208	8	y.	y.	PROPN
eurjchem-1541	208	9	;	;	PUNCT
eurjchem-1541	208	10	essassi	essassi	PROPN
eurjchem-1541	208	11	,	,	PUNCT
eurjchem-1541	208	12	e.	e.	PROPN
eurjchem-1541	208	13	m.	m.	PROPN
eurjchem-1541	208	14	;	;	PUNCT
eurjchem-1541	208	15	saadi	saadi	NOUN
eurjchem-1541	208	16	,	,	PUNCT
eurjchem-1541	208	17	m.	m.	NOUN
eurjchem-1541	208	18	;	;	PUNCT
eurjchem-1541	208	19	el	el	PROPN
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eurjchem-1541	208	21	,	,	PUNCT
eurjchem-1541	208	22	l.	l.	PROPN
eurjchem-1541	208	23	acta	acta	PROPN
eurjchem-1541	208	24	cryst	cryst	PROPN
eurjchem-1541	208	25	.	.	PUNCT
eurjchem-1541	209	1	e	e	PROPN
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eurjchem-1541	209	3	,	,	PUNCT
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eurjchem-1541	209	5	,	,	PUNCT
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eurjchem-1541	209	7	.	.	PUNCT
eurjchem-1541	210	1	[	[	X
eurjchem-1541	210	2	18	18	NUM
eurjchem-1541	210	3	]	]	PUNCT
eurjchem-1541	210	4	.	.	PUNCT
eurjchem-1541	211	1	el	el	PROPN
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eurjchem-1541	211	3	,	,	PUNCT
eurjchem-1541	211	4	m.	m.	NOUN
eurjchem-1541	211	5	;	;	PUNCT
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eurjchem-1541	211	7	,	,	PUNCT
eurjchem-1541	211	8	y.	y.	PROPN
eurjchem-1541	211	9	;	;	PUNCT
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eurjchem-1541	211	11	,	,	PUNCT
eurjchem-1541	211	12	e.	e.	PROPN
eurjchem-1541	211	13	m.	m.	PROPN
eurjchem-1541	211	14	;	;	PUNCT
eurjchem-1541	211	15	saadi	saadi	NOUN
eurjchem-1541	211	16	,	,	PUNCT
eurjchem-1541	211	17	m.	m.	NOUN
eurjchem-1541	211	18	;	;	PUNCT
eurjchem-1541	211	19	el	el	PROPN
eurjchem-1541	211	20	ammari	ammari	PROPN
eurjchem-1541	211	21	,	,	PUNCT
eurjchem-1541	211	22	l.	l.	PROPN
eurjchem-1541	211	23	acta	acta	PROPN
eurjchem-1541	211	24	cryst	cryst	PROPN
eurjchem-1541	211	25	.	.	PUNCT
eurjchem-1541	212	1	e	e	PROPN
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eurjchem-1541	212	3	,	,	PUNCT
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eurjchem-1541	212	5	,	,	PUNCT
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eurjchem-1541	212	7	.	.	PUNCT
eurjchem-1541	213	1	[	[	X
eurjchem-1541	213	2	19	19	NUM
eurjchem-1541	213	3	]	]	PUNCT
eurjchem-1541	213	4	.	.	PUNCT
eurjchem-1541	214	1	el	el	PROPN
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eurjchem-1541	214	3	,	,	PUNCT
eurjchem-1541	214	4	m.	m.	NOUN
eurjchem-1541	214	5	;	;	PUNCT
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eurjchem-1541	214	7	,	,	PUNCT
eurjchem-1541	214	8	y.	y.	PROPN
eurjchem-1541	214	9	;	;	PUNCT
eurjchem-1541	214	10	essassi	essassi	PROPN
eurjchem-1541	214	11	,	,	PUNCT
eurjchem-1541	214	12	e.	e.	PROPN
eurjchem-1541	214	13	m.	m.	PROPN
eurjchem-1541	214	14	;	;	PUNCT
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eurjchem-1541	214	16	,	,	PUNCT
eurjchem-1541	214	17	m.	m.	NOUN
eurjchem-1541	214	18	;	;	PUNCT
eurjchem-1541	214	19	el	el	PROPN
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eurjchem-1541	214	21	,	,	PUNCT
eurjchem-1541	214	22	l.	l.	PROPN
eurjchem-1541	214	23	acta	acta	PROPN
eurjchem-1541	214	24	cryst	cryst	PROPN
eurjchem-1541	214	25	.	.	PUNCT
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eurjchem-1541	215	2	2015	2015	NUM
eurjchem-1541	215	3	,	,	PUNCT
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eurjchem-1541	215	5	,	,	PUNCT
eurjchem-1541	215	6	o95‐o96	o95‐o96	PROPN
eurjchem-1541	215	7	.	.	PUNCT
eurjchem-1541	216	1	[	[	X
eurjchem-1541	216	2	20	20	NUM
eurjchem-1541	216	3	]	]	PUNCT
eurjchem-1541	216	4	.	.	PUNCT
eurjchem-1541	217	1	alsubari	alsubari	PROPN
eurjchem-1541	217	2	,	,	PUNCT
eurjchem-1541	217	3	a.	a.	NOUN
eurjchem-1541	217	4	;	;	PUNCT
eurjchem-1541	217	5	ramli	ramli	PROPN
eurjchem-1541	217	6	,	,	PUNCT
eurjchem-1541	217	7	y.	y.	PROPN
eurjchem-1541	217	8	;	;	PUNCT
eurjchem-1541	217	9	essassi	essassi	PROPN
eurjchem-1541	217	10	,	,	PUNCT
eurjchem-1541	217	11	e.	e.	PROPN
eurjchem-1541	217	12	m.	m.	PROPN
eurjchem-1541	217	13	;	;	PUNCT
eurjchem-1541	217	14	zouihri	zouihri	PROPN
eurjchem-1541	217	15	,	,	PUNCT
eurjchem-1541	217	16	h.	h.	PROPN
eurjchem-1541	217	17	acta	acta	PROPN
eurjchem-1541	217	18	cryst	cryst	PROPN
eurjchem-1541	217	19	.	.	PUNCT
eurjchem-1541	218	1	e	e	PROPN
eurjchem-1541	218	2	2011	2011	NUM
eurjchem-1541	218	3	,	,	PUNCT
eurjchem-1541	218	4	67	67	NUM
eurjchem-1541	218	5	,	,	PUNCT
eurjchem-1541	218	6	o1926‐o1926	o1926‐o1926	NOUN
eurjchem-1541	218	7	.	.	PUNCT
eurjchem-1541	219	1	[	[	X
eurjchem-1541	219	2	21	21	NUM
eurjchem-1541	219	3	]	]	PUNCT
eurjchem-1541	219	4	.	.	PUNCT
eurjchem-1541	220	1	el	el	PROPN
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eurjchem-1541	220	3	,	,	PUNCT
eurjchem-1541	220	4	m.	m.	NOUN
eurjchem-1541	220	5	;	;	PUNCT
eurjchem-1541	220	6	ramli	ramli	PROPN
eurjchem-1541	220	7	,	,	PUNCT
eurjchem-1541	220	8	y.	y.	PROPN
eurjchem-1541	220	9	;	;	PUNCT
eurjchem-1541	220	10	essassi	essassi	PROPN
eurjchem-1541	220	11	,	,	PUNCT
eurjchem-1541	220	12	e.	e.	PROPN
eurjchem-1541	220	13	m.	m.	PROPN
eurjchem-1541	220	14	;	;	PUNCT
eurjchem-1541	220	15	saadi	saadi	NOUN
eurjchem-1541	220	16	,	,	PUNCT
eurjchem-1541	220	17	m.	m.	NOUN
eurjchem-1541	220	18	;	;	PUNCT
eurjchem-1541	220	19	el	el	PROPN
eurjchem-1541	220	20	ammari	ammari	PROPN
eurjchem-1541	220	21	,	,	PUNCT
eurjchem-1541	220	22	l.	l.	PROPN
eurjchem-1541	220	23	acta	acta	PROPN
eurjchem-1541	220	24	cryst	cryst	PROPN
eurjchem-1541	220	25	.	.	PUNCT
eurjchem-1541	221	1	e	e	X
eurjchem-1541	221	2	2015	2015	NUM
eurjchem-1541	221	3	,	,	PUNCT
eurjchem-1541	221	4	71	71	NUM
eurjchem-1541	221	5	,	,	PUNCT
eurjchem-1541	221	6	o769‐o770	o769‐o770	NOUN
eurjchem-1541	221	7	.	.	PUNCT
eurjchem-1541	222	1	[	[	X
eurjchem-1541	222	2	22	22	NUM
eurjchem-1541	222	3	]	]	PUNCT
eurjchem-1541	222	4	.	.	PUNCT
eurjchem-1541	223	1	el	el	PROPN
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eurjchem-1541	223	3	m.	m.	NOUN
eurjchem-1541	223	4	;	;	PUNCT
eurjchem-1541	223	5	ramli	ramli	PROPN
eurjchem-1541	223	6	,	,	PUNCT
eurjchem-1541	223	7	y.	y.	PROPN
eurjchem-1541	223	8	;	;	PUNCT
eurjchem-1541	223	9	essassi	essassi	PROPN
eurjchem-1541	223	10	,	,	PUNCT
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eurjchem-1541	223	16	m.	m.	NOUN
eurjchem-1541	223	17	;	;	PUNCT
eurjchem-1541	223	18	el	el	PROPN
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eurjchem-1541	223	20	,	,	PUNCT
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eurjchem-1541	223	23	cryst	cryst	PROPN
eurjchem-1541	223	24	.	.	PUNCT
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eurjchem-1541	224	3	,	,	PUNCT
eurjchem-1541	224	4	70	70	NUM
eurjchem-1541	224	5	,	,	PUNCT
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eurjchem-1541	224	7	.	.	PUNCT
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eurjchem-1541	225	2	23	23	NUM
eurjchem-1541	225	3	]	]	PUNCT
eurjchem-1541	225	4	.	.	PUNCT
eurjchem-1541	226	1	el	el	PROPN
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eurjchem-1541	226	3	,	,	PUNCT
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eurjchem-1541	226	5	;	;	PUNCT
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eurjchem-1541	226	8	y.	y.	PROPN
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eurjchem-1541	226	10	zerzouf	zerzouf	PROPN
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eurjchem-1541	226	13	;	;	PUNCT
eurjchem-1541	226	14	talbaoui	talbaoui	PROPN
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eurjchem-1541	226	16	a.	a.	NOUN
eurjchem-1541	226	17	;	;	PUNCT
eurjchem-1541	226	18	bakri	bakri	NOUN
eurjchem-1541	226	19	,	,	PUNCT
eurjchem-1541	226	20	y.	y.	PROPN
eurjchem-1541	226	21	;	;	PUNCT
eurjchem-1541	226	22	essassi	essassi	PROPN
eurjchem-1541	226	23	,	,	PUNCT
eurjchem-1541	226	24	e.	e.	PROPN
eurjchem-1541	226	25	m.	m.	PROPN
eurjchem-1541	226	26	j.	j.	PROPN
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eurjchem-1541	226	30	,	,	PUNCT
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eurjchem-1541	226	35	,	,	PUNCT
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eurjchem-1541	227	3	]	]	PUNCT
eurjchem-1541	227	4	.	.	PUNCT
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eurjchem-1541	228	4	;	;	PUNCT
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eurjchem-1541	228	7	i.	i.	PROPN
eurjchem-1541	228	8	;	;	PUNCT
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eurjchem-1541	228	10	,	,	PUNCT
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eurjchem-1541	228	18	,	,	PUNCT
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eurjchem-1541	228	20	e.	e.	PROPN
eurjchem-1541	228	21	a.	a.	PROPN
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eurjchem-1541	231	2	,	,	PUNCT
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eurjchem-1541	231	8	,	,	PUNCT
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eurjchem-1541	231	13	.	.	PUNCT
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eurjchem-1541	232	5	;	;	PUNCT
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eurjchem-1541	232	7	,	,	PUNCT
eurjchem-1541	232	8	n.	n.	PROPN
eurjchem-1541	232	9	;	;	PUNCT
eurjchem-1541	232	10	hong	hong	PROPN
eurjchem-1541	232	11	,	,	PUNCT
eurjchem-1541	232	12	g.	g.	PROPN
eurjchem-1541	232	13	;	;	PUNCT
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eurjchem-1541	232	15	,	,	PUNCT
eurjchem-1541	232	16	j.	j.	PROPN
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eurjchem-1541	233	2	,	,	PUNCT
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eurjchem-1541	233	4	,	,	PUNCT
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eurjchem-1541	234	3	]	]	PUNCT
eurjchem-1541	234	4	.	.	PUNCT
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eurjchem-1541	235	2	,	,	PUNCT
eurjchem-1541	235	3	p.	p.	NOUN
eurjchem-1541	235	4	drugs	drug	NOUN
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eurjchem-1541	235	6	,	,	PUNCT
eurjchem-1541	235	7	44	44	NUM
eurjchem-1541	235	8	,	,	PUNCT
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eurjchem-1541	235	10	.	.	PUNCT
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eurjchem-1541	237	1	j.	j.	PROPN
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