id	sid	tid	token	lemma	pos
eurjchem-1596	1	1	untitled	untitle	VERB
eurjchem-1596	1	2	european	european	PROPN
eurjchem-1596	1	3	journal	journal	PROPN
eurjchem-1596	1	4	of	of	ADP
eurjchem-1596	1	5	chemistry	chemistry	NOUN
eurjchem-1596	1	6	8	8	NUM
eurjchem-1596	1	7	(	(	PUNCT
eurjchem-1596	1	8	3	3	NUM
eurjchem-1596	1	9	)	)	PUNCT
eurjchem-1596	1	10	(	(	PUNCT
eurjchem-1596	1	11	2017	2017	NUM
eurjchem-1596	1	12	)	)	PUNCT
eurjchem-1596	1	13	258‐264	258‐264	NUM
eurjchem-1596	1	14	european	european	ADJ
eurjchem-1596	1	15	journal	journal	NOUN
eurjchem-1596	1	16	of	of	ADP
eurjchem-1596	1	17	chemistry	chemistry	NOUN
eurjchem-1596	1	18	issn	issn	PROPN
eurjchem-1596	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-1596	1	20	(	(	PUNCT
eurjchem-1596	1	21	print	print	NOUN
eurjchem-1596	1	22	)	)	PUNCT
eurjchem-1596	1	23	/	/	SYM
eurjchem-1596	1	24	issn	issn	PROPN
eurjchem-1596	1	25	2153‐2257	2153‐2257	NUM
eurjchem-1596	1	26	(	(	PUNCT
eurjchem-1596	1	27	online	online	ADJ
eurjchem-1596	1	28	)	)	PUNCT
eurjchem-1596	1	29			NOUN
eurjchem-1596	1	30	2017	2017	NUM
eurjchem-1596	1	31	atlanta	atlanta	PROPN
eurjchem-1596	1	32	publishing	publishing	PROPN
eurjchem-1596	1	33	house	house	PROPN
eurjchem-1596	1	34	llc	llc	PROPN
eurjchem-1596	1	35	‐	‐	PUNCT
eurjchem-1596	1	36	all	all	DET
eurjchem-1596	1	37	rights	right	NOUN
eurjchem-1596	1	38	reserved	reserve	VERB
eurjchem-1596	1	39	‐	‐	NOUN
eurjchem-1596	1	40	printed	print	VERB
eurjchem-1596	1	41	in	in	ADP
eurjchem-1596	1	42	the	the	DET
eurjchem-1596	1	43	usa	usa	PROPN
eurjchem-1596	1	44	http://dx.doi.org/10.5155/eurjchem.8.3.258-264.1596	http://dx.doi.org/10.5155/eurjchem.8.3.258-264.1596	PROPN
eurjchem-1596	1	45	european	european	PROPN
eurjchem-1596	1	46	journal	journal	PROPN
eurjchem-1596	1	47	of	of	ADP
eurjchem-1596	1	48	chemistry	chemistry	PROPN
eurjchem-1596	1	49	journal	journal	PROPN
eurjchem-1596	1	50	webpage	webpage	NOUN
eurjchem-1596	1	51	:	:	PUNCT
eurjchem-1596	1	52	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1596	1	53	rapid	rapid	ADJ
eurjchem-1596	1	54	and	and	CCONJ
eurjchem-1596	1	55	sensitive	sensitive	ADJ
eurjchem-1596	1	56	determination	determination	NOUN
eurjchem-1596	1	57	of	of	ADP
eurjchem-1596	1	58	selective	selective	ADJ
eurjchem-1596	1	59	progesterone	progesterone	NOUN
eurjchem-1596	1	60	modulator	modulator	NOUN
eurjchem-1596	1	61	ulipristal	ulipristal	ADJ
eurjchem-1596	1	62	acetate	acetate	NOUN
eurjchem-1596	1	63	in	in	ADP
eurjchem-1596	1	64	human	human	ADJ
eurjchem-1596	1	65	plasma	plasma	NOUN
eurjchem-1596	1	66	nagaraju	nagaraju	PROPN
eurjchem-1596	1	67	pappula	pappula	NOUN
eurjchem-1596	1	68	1	1	NUM
eurjchem-1596	1	69	,	,	PUNCT
eurjchem-1596	1	70	*	*	PROPN
eurjchem-1596	1	71	,	,	PUNCT
eurjchem-1596	1	72	balaji	balaji	PROPN
eurjchem-1596	1	73	kodali	kodali	PROPN
eurjchem-1596	1	74	2	2	NUM
eurjchem-1596	1	75	and	and	CCONJ
eurjchem-1596	1	76	peda	peda	PROPN
eurjchem-1596	1	77	varma	varma	PROPN
eurjchem-1596	1	78	datla	datla	VERB
eurjchem-1596	1	79	3	3	NUM
eurjchem-1596	1	80	1	1	NUM
eurjchem-1596	1	81	department	department	NOUN
eurjchem-1596	1	82	of	of	ADP
eurjchem-1596	1	83	pharmaceutical	pharmaceutical	ADJ
eurjchem-1596	1	84	analysis	analysis	NOUN
eurjchem-1596	1	85	,	,	PUNCT
eurjchem-1596	1	86	hindu	hindu	NOUN
eurjchem-1596	1	87	college	college	NOUN
eurjchem-1596	1	88	of	of	ADP
eurjchem-1596	1	89	pharmacy	pharmacy	NOUN
eurjchem-1596	1	90	,	,	PUNCT
eurjchem-1596	1	91	guntur‐522002	guntur‐522002	PROPN
eurjchem-1596	1	92	,	,	PUNCT
eurjchem-1596	1	93	andhra	andhra	PROPN
eurjchem-1596	1	94	pradesh	pradesh	PROPN
eurjchem-1596	1	95	,	,	PUNCT
eurjchem-1596	1	96	india	india	PROPN
eurjchem-1596	1	97	2	2	NUM
eurjchem-1596	1	98	college	college	NOUN
eurjchem-1596	1	99	of	of	ADP
eurjchem-1596	1	100	pharmaceutical	pharmaceutical	NOUN
eurjchem-1596	1	101	sciences	science	NOUN
eurjchem-1596	1	102	,	,	PUNCT
eurjchem-1596	1	103	acharya	acharya	PROPN
eurjchem-1596	1	104	nagarjuna	nagarjuna	PROPN
eurjchem-1596	1	105	university	university	PROPN
eurjchem-1596	1	106	,	,	PUNCT
eurjchem-1596	1	107	nagarjuna	nagarjuna	PROPN
eurjchem-1596	1	108	nagar‐522510	nagar‐522510	PROPN
eurjchem-1596	1	109	,	,	PUNCT
eurjchem-1596	1	110	guntur	guntur	PROPN
eurjchem-1596	1	111	(	(	PUNCT
eurjchem-1596	1	112	dist	dist	NOUN
eurjchem-1596	1	113	)	)	PUNCT
eurjchem-1596	1	114	,	,	PUNCT
eurjchem-1596	1	115	andhra	andhra	PROPN
eurjchem-1596	1	116	pradesh	pradesh	PROPN
eurjchem-1596	1	117	,	,	PUNCT
eurjchem-1596	1	118	india	india	PROPN
eurjchem-1596	1	119	3	3	NUM
eurjchem-1596	1	120	clinical	clinical	ADJ
eurjchem-1596	1	121	pharmacology	pharmacology	NOUN
eurjchem-1596	1	122	and	and	CCONJ
eurjchem-1596	1	123	bio	bio	PROPN
eurjchem-1596	1	124	sciences	sciences	PROPN
eurjchem-1596	1	125	division	division	PROPN
eurjchem-1596	1	126	,	,	PUNCT
eurjchem-1596	1	127	ra	ra	PROPN
eurjchem-1596	1	128	chem	chem	PROPN
eurjchem-1596	1	129	pharma	pharma	PROPN
eurjchem-1596	1	130	ltd	ltd	PROPN
eurjchem-1596	1	131	.	.	PROPN
eurjchem-1596	1	132	,	,	PUNCT
eurjchem-1596	1	133	hyderabad	hyderabad	PROPN
eurjchem-1596	1	134	,	,	PUNCT
eurjchem-1596	1	135	500037	500037	NUM
eurjchem-1596	1	136	,	,	PUNCT
eurjchem-1596	1	137	india	india	PROPN
eurjchem-1596	1	138	*	*	PUNCT
eurjchem-1596	1	139	corresponding	correspond	VERB
eurjchem-1596	1	140	author	author	NOUN
eurjchem-1596	1	141	at	at	ADP
eurjchem-1596	1	142	:	:	PUNCT
eurjchem-1596	1	143	department	department	NOUN
eurjchem-1596	1	144	of	of	ADP
eurjchem-1596	1	145	pharmaceutical	pharmaceutical	ADJ
eurjchem-1596	1	146	analysis	analysis	NOUN
eurjchem-1596	1	147	,	,	PUNCT
eurjchem-1596	1	148	hindu	hindu	NOUN
eurjchem-1596	1	149	college	college	NOUN
eurjchem-1596	1	150	of	of	ADP
eurjchem-1596	1	151	pharmacy	pharmacy	NOUN
eurjchem-1596	1	152	,	,	PUNCT
eurjchem-1596	1	153	guntur‐522002	guntur‐522002	PROPN
eurjchem-1596	1	154	,	,	PUNCT
eurjchem-1596	1	155	andhra	andhra	PROPN
eurjchem-1596	1	156	pradesh	pradesh	PROPN
eurjchem-1596	1	157	,	,	PUNCT
eurjchem-1596	1	158	india	india	PROPN
eurjchem-1596	1	159	.	.	PUNCT
eurjchem-1596	2	1	tel	tel	PROPN
eurjchem-1596	2	2	.	.	PUNCT
eurjchem-1596	2	3	:	:	PUNCT
eurjchem-1596	3	1	+91.998.5304304	+91.998.5304304	X
eurjchem-1596	3	2	.	.	X
eurjchem-1596	3	3	fax	fax	NOUN
eurjchem-1596	3	4	:	:	PUNCT
eurjchem-1596	3	5	+91.998.5304304	+91.998.5304304	PROPN
eurjchem-1596	3	6	.	.	PUNCT
eurjchem-1596	3	7	e‐mail	e‐mail	PUNCT
eurjchem-1596	4	1	address	address	NOUN
eurjchem-1596	4	2	:	:	PUNCT
eurjchem-1596	4	3	pappulanagaraju@gmail.com	pappulanagaraju@gmail.com	X
eurjchem-1596	4	4	(	(	PUNCT
eurjchem-1596	4	5	n.	n.	NOUN
eurjchem-1596	4	6	pappula	pappula	PROPN
eurjchem-1596	4	7	)	)	PUNCT
eurjchem-1596	4	8	.	.	PUNCT
eurjchem-1596	5	1	article	article	NOUN
eurjchem-1596	5	2	information	information	PROPN
eurjchem-1596	5	3	abstract	abstract	ADJ
eurjchem-1596	5	4	doi	doi	PROPN
eurjchem-1596	5	5	:	:	PUNCT
eurjchem-1596	5	6	 	 	SPACE
eurjchem-1596	5	7	10.5155	10.5155	NUM
eurjchem-1596	5	8	/	/	SYM
eurjchem-1596	5	9	eurjchem.8.3.258	eurjchem.8.3.258	PROPN
eurjchem-1596	5	10	-	-	PUNCT
eurjchem-1596	5	11	264.1596	264.1596	NUM
eurjchem-1596	5	12	received	receive	VERB
eurjchem-1596	5	13	:	:	PUNCT
eurjchem-1596	5	14	12	12	NUM
eurjchem-1596	5	15	june	june	PROPN
eurjchem-1596	5	16	2017	2017	NUM
eurjchem-1596	5	17	received	receive	VERB
eurjchem-1596	5	18	in	in	ADP
eurjchem-1596	5	19	revised	revise	VERB
eurjchem-1596	5	20	form	form	NOUN
eurjchem-1596	5	21	:	:	PUNCT
eurjchem-1596	5	22	05	05	NUM
eurjchem-1596	5	23	august	august	PROPN
eurjchem-1596	5	24	2017	2017	NUM
eurjchem-1596	5	25	accepted	accept	VERB
eurjchem-1596	5	26	:	:	PUNCT
eurjchem-1596	5	27	05	05	NUM
eurjchem-1596	5	28	august	august	PROPN
eurjchem-1596	5	29	2017	2017	NUM
eurjchem-1596	5	30	published	publish	VERB
eurjchem-1596	5	31	online	online	ADV
eurjchem-1596	5	32	:	:	PUNCT
eurjchem-1596	5	33	30	30	NUM
eurjchem-1596	5	34	september	september	PROPN
eurjchem-1596	5	35	2017	2017	NUM
eurjchem-1596	5	36	printed	print	VERB
eurjchem-1596	5	37	:	:	PUNCT
eurjchem-1596	5	38	30	30	NUM
eurjchem-1596	5	39	september	september	PROPN
eurjchem-1596	5	40	2017	2017	NUM
eurjchem-1596	5	41	  	  	SPACE
eurjchem-1596	5	42	ulipristal	ulipristal	ADJ
eurjchem-1596	5	43	acetate	acetate	NOUN
eurjchem-1596	5	44	is	be	AUX
eurjchem-1596	5	45	a	a	DET
eurjchem-1596	5	46	new	new	ADJ
eurjchem-1596	5	47	synthetic	synthetic	ADJ
eurjchem-1596	5	48	selective	selective	ADJ
eurjchem-1596	5	49	progesterone	progesterone	NOUN
eurjchem-1596	5	50	receptor	receptor	NOUN
eurjchem-1596	5	51	modulator	modulator	NOUN
eurjchem-1596	5	52	developed	develop	VERB
eurjchem-1596	5	53	mainly	mainly	ADV
eurjchem-1596	5	54	as	as	ADP
eurjchem-1596	5	55	emergency	emergency	NOUN
eurjchem-1596	5	56	contraceptive	contraceptive	NOUN
eurjchem-1596	5	57	(	(	PUNCT
eurjchem-1596	5	58	ec	ec	PROPN
eurjchem-1596	5	59	)	)	PUNCT
eurjchem-1596	5	60	and	and	CCONJ
eurjchem-1596	5	61	also	also	ADV
eurjchem-1596	5	62	used	use	VERB
eurjchem-1596	5	63	for	for	ADP
eurjchem-1596	5	64	the	the	DET
eurjchem-1596	5	65	treatment	treatment	NOUN
eurjchem-1596	5	66	of	of	ADP
eurjchem-1596	5	67	uterine	uterine	ADJ
eurjchem-1596	5	68	fibroids	fibroid	NOUN
eurjchem-1596	5	69	.	.	PUNCT
eurjchem-1596	6	1	a	a	DET
eurjchem-1596	6	2	cost	cost	NOUN
eurjchem-1596	6	3	effective	effective	ADJ
eurjchem-1596	6	4	,	,	PUNCT
eurjchem-1596	6	5	sensitive	sensitive	ADJ
eurjchem-1596	6	6	,	,	PUNCT
eurjchem-1596	6	7	simple	simple	ADJ
eurjchem-1596	6	8	and	and	CCONJ
eurjchem-1596	6	9	rapid	rapid	ADJ
eurjchem-1596	6	10	high	high	ADJ
eurjchem-1596	6	11	performance	performance	NOUN
eurjchem-1596	6	12	liquid	liquid	VERB
eurjchem-1596	6	13	chromatography‐tandem	chromatography‐tandem	PROPN
eurjchem-1596	6	14	mass	mass	NOUN
eurjchem-1596	6	15	spectrometry	spectrometry	NOUN
eurjchem-1596	6	16	(	(	PUNCT
eurjchem-1596	6	17	lc‐ms	lc‐ms	NUM
eurjchem-1596	6	18	/	/	SYM
eurjchem-1596	6	19	ms	ms	PROPN
eurjchem-1596	6	20	)	)	PUNCT
eurjchem-1596	6	21	method	method	NOUN
eurjchem-1596	6	22	was	be	AUX
eurjchem-1596	6	23	developed	develop	VERB
eurjchem-1596	6	24	and	and	CCONJ
eurjchem-1596	6	25	validated	validate	VERB
eurjchem-1596	6	26	for	for	ADP
eurjchem-1596	6	27	the	the	DET
eurjchem-1596	6	28	analysis	analysis	NOUN
eurjchem-1596	6	29	of	of	ADP
eurjchem-1596	6	30	ulipristal	ulipristal	ADJ
eurjchem-1596	6	31	acetate	acetate	NOUN
eurjchem-1596	6	32	in	in	ADP
eurjchem-1596	6	33	human	human	ADJ
eurjchem-1596	6	34	plasma	plasma	NOUN
eurjchem-1596	6	35	.	.	PUNCT
eurjchem-1596	7	1	following	follow	VERB
eurjchem-1596	7	2	liquid‐liquid	liquid‐liquid	PROPN
eurjchem-1596	7	3	extraction	extraction	NOUN
eurjchem-1596	7	4	,	,	PUNCT
eurjchem-1596	7	5	the	the	DET
eurjchem-1596	7	6	analyte	analyte	NOUN
eurjchem-1596	7	7	(	(	PUNCT
eurjchem-1596	7	8	ulipristal	ulipristal	ADJ
eurjchem-1596	7	9	acetate	acetate	NOUN
eurjchem-1596	7	10	)	)	PUNCT
eurjchem-1596	7	11	and	and	CCONJ
eurjchem-1596	7	12	internal	internal	ADJ
eurjchem-1596	7	13	standard	standard	ADJ
eurjchem-1596	7	14	(	(	PUNCT
eurjchem-1596	7	15	levonorgestrel	levonorgestrel	NOUN
eurjchem-1596	7	16	)	)	PUNCT
eurjchem-1596	7	17	were	be	AUX
eurjchem-1596	7	18	chromatographed	chromatographe	VERB
eurjchem-1596	7	19	using	use	VERB
eurjchem-1596	7	20	mobile	mobile	ADJ
eurjchem-1596	7	21	phase	phase	NOUN
eurjchem-1596	7	22	in	in	ADP
eurjchem-1596	7	23	an	an	DET
eurjchem-1596	7	24	isocratic	isocratic	ADJ
eurjchem-1596	7	25	elution	elution	NOUN
eurjchem-1596	7	26	mode	mode	NOUN
eurjchem-1596	7	27	on	on	ADP
eurjchem-1596	7	28	a	a	DET
eurjchem-1596	7	29	reverse	reverse	ADJ
eurjchem-1596	7	30	phase	phase	NOUN
eurjchem-1596	7	31	c18	c18	NOUN
eurjchem-1596	7	32	column	column	PROPN
eurjchem-1596	7	33	.	.	PUNCT
eurjchem-1596	8	1	the	the	DET
eurjchem-1596	8	2	lc‐ms	lc‐ms	NUM
eurjchem-1596	8	3	/	/	SYM
eurjchem-1596	8	4	ms	ms	PROPN
eurjchem-1596	8	5	operated	operate	VERB
eurjchem-1596	8	6	in	in	ADP
eurjchem-1596	8	7	multiple	multiple	ADJ
eurjchem-1596	8	8	reaction	reaction	NOUN
eurjchem-1596	8	9	monitoring	monitor	VERB
eurjchem-1596	8	10	mode	mode	NOUN
eurjchem-1596	8	11	for	for	ADP
eurjchem-1596	8	12	respective	respective	ADJ
eurjchem-1596	8	13	[	[	X
eurjchem-1596	8	14	m+h]+	m+h]+	PROPN
eurjchem-1596	8	15	ions	ion	NOUN
eurjchem-1596	8	16	,	,	PUNCT
eurjchem-1596	8	17	m	m	PROPN
eurjchem-1596	8	18	/	/	SYM
eurjchem-1596	8	19	z	z	NOUN
eurjchem-1596	8	20	476.2/134.1	476.2/134.1	NUM
eurjchem-1596	8	21	for	for	ADP
eurjchem-1596	8	22	analyte	analyte	NOUN
eurjchem-1596	8	23	and	and	CCONJ
eurjchem-1596	8	24	313.3/245.1	313.3/245.1	NUM
eurjchem-1596	8	25	for	for	ADP
eurjchem-1596	8	26	internal	internal	ADJ
eurjchem-1596	8	27	standard	standard	NOUN
eurjchem-1596	8	28	.	.	PUNCT
eurjchem-1596	9	1	the	the	DET
eurjchem-1596	9	2	assay	assay	NOUN
eurjchem-1596	9	3	exhibited	exhibit	VERB
eurjchem-1596	9	4	linear	linear	ADJ
eurjchem-1596	9	5	dynamic	dynamic	ADJ
eurjchem-1596	9	6	range	range	NOUN
eurjchem-1596	9	7	of	of	ADP
eurjchem-1596	9	8	1‐300	1‐300	NUM
eurjchem-1596	9	9	ng	ng	PROPN
eurjchem-1596	9	10	/	/	SYM
eurjchem-1596	9	11	ml	ml	PROPN
eurjchem-1596	9	12	.	.	PUNCT
eurjchem-1596	10	1	the	the	DET
eurjchem-1596	10	2	lower	low	ADJ
eurjchem-1596	10	3	limit	limit	NOUN
eurjchem-1596	10	4	of	of	ADP
eurjchem-1596	10	5	quantification	quantification	NOUN
eurjchem-1596	10	6	was	be	AUX
eurjchem-1596	10	7	1	1	NUM
eurjchem-1596	10	8	ng	ng	NOUN
eurjchem-1596	10	9	/	/	SYM
eurjchem-1596	10	10	ml	ml	NOUN
eurjchem-1596	10	11	with	with	ADP
eurjchem-1596	10	12	relative	relative	ADJ
eurjchem-1596	10	13	standard	standard	ADJ
eurjchem-1596	10	14	deviation	deviation	NOUN
eurjchem-1596	10	15	of	of	ADP
eurjchem-1596	10	16	7.0	7.0	NUM
eurjchem-1596	10	17	%	%	NOUN
eurjchem-1596	10	18	.	.	PUNCT
eurjchem-1596	11	1	the	the	DET
eurjchem-1596	11	2	intra‐batch	intra‐batch	NOUN
eurjchem-1596	11	3	and	and	CCONJ
eurjchem-1596	11	4	inter‐batch	inter‐batch	NOUN
eurjchem-1596	11	5	results	result	NOUN
eurjchem-1596	11	6	were	be	AUX
eurjchem-1596	11	7	precise	precise	ADJ
eurjchem-1596	11	8	with	with	ADP
eurjchem-1596	11	9	coefficient	coefficient	NOUN
eurjchem-1596	11	10	variation	variation	NOUN
eurjchem-1596	11	11	of	of	ADP
eurjchem-1596	11	12	2.7	2.7	NUM
eurjchem-1596	11	13	to	to	PART
eurjchem-1596	11	14	7.0	7.0	NUM
eurjchem-1596	11	15	(	(	PUNCT
eurjchem-1596	11	16	%	%	NOUN
eurjchem-1596	11	17	)	)	PUNCT
eurjchem-1596	11	18	and	and	CCONJ
eurjchem-1596	11	19	accuracy	accuracy	NOUN
eurjchem-1596	11	20	of	of	ADP
eurjchem-1596	11	21	94.2‐99.8	94.2‐99.8	NUM
eurjchem-1596	11	22	(	(	PUNCT
eurjchem-1596	11	23	%	%	NOUN
eurjchem-1596	11	24	)	)	PUNCT
eurjchem-1596	11	25	.	.	PUNCT
eurjchem-1596	12	1	the	the	DET
eurjchem-1596	12	2	validated	validate	VERB
eurjchem-1596	12	3	method	method	NOUN
eurjchem-1596	12	4	was	be	AUX
eurjchem-1596	12	5	simple	simple	ADJ
eurjchem-1596	12	6	,	,	PUNCT
eurjchem-1596	12	7	fast	fast	ADJ
eurjchem-1596	12	8	and	and	CCONJ
eurjchem-1596	12	9	repeatable	repeatable	ADJ
eurjchem-1596	12	10	for	for	ADP
eurjchem-1596	12	11	bioequivalence	bioequivalence	NOUN
eurjchem-1596	12	12	,	,	PUNCT
eurjchem-1596	12	13	pharmacokinetic	pharmacokinetic	ADJ
eurjchem-1596	12	14	and	and	CCONJ
eurjchem-1596	12	15	therapeutic	therapeutic	ADJ
eurjchem-1596	12	16	monitoring	monitoring	NOUN
eurjchem-1596	12	17	studies	study	NOUN
eurjchem-1596	12	18	.	.	PUNCT
eurjchem-1596	13	1	keywords	keyword	VERB
eurjchem-1596	13	2	lc	lc	PROPN
eurjchem-1596	13	3	/	/	SYM
eurjchem-1596	13	4	ms	ms	PROPN
eurjchem-1596	13	5	human	human	PROPN
eurjchem-1596	13	6	plasma	plasma	PROPN
eurjchem-1596	13	7	ulipristal	ulipristal	PROPN
eurjchem-1596	13	8	acetate	acetate	PROPN
eurjchem-1596	13	9	istd	istd	PROPN
eurjchem-1596	13	10	trend	trend	NOUN
eurjchem-1596	13	11	analysis	analysis	NOUN
eurjchem-1596	14	1	oral	oral	ADJ
eurjchem-1596	14	2	contraceptives	contraceptive	NOUN
eurjchem-1596	14	3	liquid‐liquid	liquid‐liquid	ADJ
eurjchem-1596	14	4	extraction	extraction	NOUN
eurjchem-1596	14	5	cite	cite	VERB
eurjchem-1596	14	6	this	this	PRON
eurjchem-1596	14	7	:	:	PUNCT
eurjchem-1596	14	8	eur	eur	PROPN
eurjchem-1596	14	9	.	.	PUNCT
eurjchem-1596	15	1	j.	j.	PROPN
eurjchem-1596	15	2	chem	chem	PROPN
eurjchem-1596	15	3	.	.	PUNCT
eurjchem-1596	16	1	2017	2017	NUM
eurjchem-1596	16	2	,	,	PUNCT
eurjchem-1596	16	3	8(3	8(3	NUM
eurjchem-1596	16	4	)	)	PUNCT
eurjchem-1596	16	5	,	,	PUNCT
eurjchem-1596	16	6	258‐264	258‐264	NUM
eurjchem-1596	16	7	1	1	NUM
eurjchem-1596	16	8	.	.	PUNCT
eurjchem-1596	16	9	introduction	introduction	NOUN
eurjchem-1596	16	10	despite	despite	SCONJ
eurjchem-1596	16	11	the	the	DET
eurjchem-1596	16	12	availability	availability	NOUN
eurjchem-1596	16	13	of	of	ADP
eurjchem-1596	16	14	highly	highly	ADV
eurjchem-1596	16	15	effective	effective	ADJ
eurjchem-1596	16	16	methods	method	NOUN
eurjchem-1596	16	17	of	of	ADP
eurjchem-1596	16	18	contraception	contraception	NOUN
eurjchem-1596	16	19	,	,	PUNCT
eurjchem-1596	16	20	a	a	DET
eurjchem-1596	16	21	great	great	ADJ
eurjchem-1596	16	22	number	number	NOUN
eurjchem-1596	16	23	of	of	ADP
eurjchem-1596	16	24	pregnancies	pregnancy	NOUN
eurjchem-1596	16	25	are	be	AUX
eurjchem-1596	16	26	unintended	unintended	ADJ
eurjchem-1596	16	27	.	.	PUNCT
eurjchem-1596	17	1	many	many	ADJ
eurjchem-1596	17	2	women	woman	NOUN
eurjchem-1596	17	3	who	who	PRON
eurjchem-1596	17	4	experience	experience	VERB
eurjchem-1596	17	5	an	an	DET
eurjchem-1596	17	6	unintended	unintended	ADJ
eurjchem-1596	17	7	pregnancy	pregnancy	NOUN
eurjchem-1596	17	8	have	have	AUX
eurjchem-1596	17	9	become	become	VERB
eurjchem-1596	17	10	pregnant	pregnant	ADJ
eurjchem-1596	17	11	as	as	ADP
eurjchem-1596	17	12	a	a	DET
eurjchem-1596	17	13	result	result	NOUN
eurjchem-1596	17	14	of	of	ADP
eurjchem-1596	17	15	either	either	CCONJ
eurjchem-1596	17	16	lacking	lack	VERB
eurjchem-1596	17	17	of	of	ADP
eurjchem-1596	17	18	contraceptives	contraceptive	NOUN
eurjchem-1596	17	19	or	or	CCONJ
eurjchem-1596	17	20	contraceptive	contraceptive	ADJ
eurjchem-1596	17	21	failure	failure	NOUN
eurjchem-1596	17	22	.	.	PUNCT
eurjchem-1596	18	1	emergency	emergency	NOUN
eurjchem-1596	18	2	contraception	contraception	NOUN
eurjchem-1596	18	3	is	be	AUX
eurjchem-1596	18	4	defined	define	VERB
eurjchem-1596	18	5	as	as	ADP
eurjchem-1596	18	6	the	the	DET
eurjchem-1596	18	7	use	use	NOUN
eurjchem-1596	18	8	of	of	ADP
eurjchem-1596	18	9	any	any	DET
eurjchem-1596	18	10	drug	drug	NOUN
eurjchem-1596	18	11	or	or	CCONJ
eurjchem-1596	18	12	device	device	NOUN
eurjchem-1596	18	13	after	after	ADP
eurjchem-1596	18	14	unprotected	unprotected	ADJ
eurjchem-1596	18	15	intercourse	intercourse	NOUN
eurjchem-1596	18	16	to	to	PART
eurjchem-1596	18	17	prevent	prevent	VERB
eurjchem-1596	18	18	an	an	DET
eurjchem-1596	18	19	unwanted	unwanted	ADJ
eurjchem-1596	18	20	pregnancy	pregnancy	NOUN
eurjchem-1596	18	21	.	.	PUNCT
eurjchem-1596	19	1	ulipristal	ulipristal	ADJ
eurjchem-1596	19	2	acetate	acetate	PROPN
eurjchem-1596	19	3	is	be	AUX
eurjchem-1596	19	4	a	a	DET
eurjchem-1596	19	5	derivative	derivative	NOUN
eurjchem-1596	19	6	of	of	ADP
eurjchem-1596	19	7	19‐norprogesterone	19‐norprogesterone	NUM
eurjchem-1596	19	8	and	and	CCONJ
eurjchem-1596	19	9	was	be	AUX
eurjchem-1596	19	10	developed	develop	VERB
eurjchem-1596	19	11	to	to	PART
eurjchem-1596	19	12	have	have	AUX
eurjchem-1596	19	13	enhanced	enhance	VERB
eurjchem-1596	19	14	specificity	specificity	NOUN
eurjchem-1596	19	15	for	for	ADP
eurjchem-1596	19	16	progesterone	progesterone	NOUN
eurjchem-1596	19	17	receptor	receptor	NOUN
eurjchem-1596	19	18	.	.	PUNCT
eurjchem-1596	20	1	pre‐clinical	pre‐clinical	ADJ
eurjchem-1596	20	2	studies	study	NOUN
eurjchem-1596	20	3	indicate	indicate	VERB
eurjchem-1596	20	4	that	that	SCONJ
eurjchem-1596	20	5	ulipristal	ulipristal	ADJ
eurjchem-1596	20	6	acetate	acetate	NOUN
eurjchem-1596	20	7	(	(	PUNCT
eurjchem-1596	20	8	upa	upa	NOUN
eurjchem-1596	20	9	)	)	PUNCT
eurjchem-1596	20	10	binds	bind	VERB
eurjchem-1596	20	11	to	to	ADP
eurjchem-1596	20	12	human	human	ADJ
eurjchem-1596	20	13	progesterone	progesterone	NOUN
eurjchem-1596	20	14	,	,	PUNCT
eurjchem-1596	20	15	glucocorticoid	glucocorticoid	NOUN
eurjchem-1596	20	16	and	and	CCONJ
eurjchem-1596	20	17	androgen	androgen	NOUN
eurjchem-1596	20	18	receptors	receptor	NOUN
eurjchem-1596	20	19	at	at	ADP
eurjchem-1596	20	20	app‐	app‐	PRON
eurjchem-1596	20	21	roximately	roximately	ADV
eurjchem-1596	20	22	6	6	NUM
eurjchem-1596	20	23	,	,	PUNCT
eurjchem-1596	20	24	1.5	1.5	NUM
eurjchem-1596	20	25	and	and	CCONJ
eurjchem-1596	20	26	0.2	0.2	NUM
eurjchem-1596	20	27	times	time	NOUN
eurjchem-1596	20	28	the	the	DET
eurjchem-1596	20	29	affinity	affinity	NOUN
eurjchem-1596	20	30	of	of	ADP
eurjchem-1596	20	31	the	the	DET
eurjchem-1596	20	32	endogenous	endogenous	ADJ
eurjchem-1596	20	33	ligands	ligand	NOUN
eurjchem-1596	20	34	and	and	CCONJ
eurjchem-1596	20	35	shows	show	VERB
eurjchem-1596	20	36	in‐vivo	in‐vivo	ADJ
eurjchem-1596	20	37	anti‐glucocorticoid	anti‐glucocorticoid	NOUN
eurjchem-1596	20	38	and	and	CCONJ
eurjchem-1596	20	39	anti‐	anti‐	NOUN
eurjchem-1596	20	40	androgen	androgen	NOUN
eurjchem-1596	20	41	activity	activity	NOUN
eurjchem-1596	20	42	at	at	ADP
eurjchem-1596	20	43	doses	dose	NOUN
eurjchem-1596	20	44	approximately	approximately	ADV
eurjchem-1596	20	45	50‐fold	50‐fold	NUM
eurjchem-1596	20	46	greater	great	ADJ
eurjchem-1596	20	47	than	than	ADP
eurjchem-1596	20	48	those	those	PRON
eurjchem-1596	20	49	needed	need	VERB
eurjchem-1596	20	50	for	for	ADP
eurjchem-1596	20	51	anti‐progestin	anti‐progestin	AUX
eurjchem-1596	20	52	effect	effect	VERB
eurjchem-1596	20	53	[	[	X
eurjchem-1596	20	54	1	1	NUM
eurjchem-1596	20	55	]	]	PUNCT
eurjchem-1596	20	56	.	.	PUNCT
eurjchem-1596	21	1	the	the	DET
eurjchem-1596	21	2	drug	drug	NOUN
eurjchem-1596	21	3	has	have	VERB
eurjchem-1596	21	4	minimal	minimal	ADJ
eurjchem-1596	21	5	affinity	affinity	NOUN
eurjchem-1596	21	6	to	to	ADP
eurjchem-1596	21	7	androgen	androgen	NOUN
eurjchem-1596	21	8	receptor	receptor	NOUN
eurjchem-1596	21	9	and	and	CCONJ
eurjchem-1596	21	10	no	no	DET
eurjchem-1596	21	11	affinity	affinity	NOUN
eurjchem-1596	21	12	to	to	ADP
eurjchem-1596	21	13	human	human	ADJ
eurjchem-1596	21	14	estrogenic	estrogenic	NOUN
eurjchem-1596	21	15	or	or	CCONJ
eurjchem-1596	21	16	mineralocorticoid	mineralocorticoid	NOUN
eurjchem-1596	21	17	receptors	receptor	NOUN
eurjchem-1596	21	18	[	[	X
eurjchem-1596	21	19	2	2	NUM
eurjchem-1596	21	20	]	]	PUNCT
eurjchem-1596	21	21	.	.	PUNCT
eurjchem-1596	22	1	ulipristal	ulipristal	ADJ
eurjchem-1596	22	2	acetate	acetate	PROPN
eurjchem-1596	22	3	is	be	AUX
eurjchem-1596	22	4	new	new	ADJ
eurjchem-1596	22	5	drug	drug	NOUN
eurjchem-1596	22	6	for	for	ADP
eurjchem-1596	22	7	ec	ec	PROPN
eurjchem-1596	22	8	,	,	PUNCT
eurjchem-1596	22	9	approved	approve	VERB
eurjchem-1596	22	10	and	and	CCONJ
eurjchem-1596	22	11	marke‐	marke‐	NOUN
eurjchem-1596	22	12	ted	te	VERB
eurjchem-1596	22	13	in	in	ADP
eurjchem-1596	22	14	united	united	PROPN
eurjchem-1596	22	15	states	states	PROPN
eurjchem-1596	22	16	,	,	PUNCT
eurjchem-1596	22	17	european	european	PROPN
eurjchem-1596	22	18	union	union	PROPN
eurjchem-1596	22	19	and	and	CCONJ
eurjchem-1596	22	20	latin	latin	ADJ
eurjchem-1596	22	21	american	american	ADJ
eurjchem-1596	22	22	countries	country	NOUN
eurjchem-1596	22	23	.	.	PUNCT
eurjchem-1596	23	1	it	it	PRON
eurjchem-1596	23	2	is	be	AUX
eurjchem-1596	23	3	administered	administer	VERB
eurjchem-1596	23	4	as	as	ADP
eurjchem-1596	23	5	a	a	DET
eurjchem-1596	23	6	one‐time	one‐time	NUM
eurjchem-1596	23	7	30	30	NUM
eurjchem-1596	23	8	mg	mg	NOUN
eurjchem-1596	23	9	dose	dose	VERB
eurjchem-1596	23	10	within	within	ADP
eurjchem-1596	23	11	120	120	NUM
eurjchem-1596	23	12	hours	hour	NOUN
eurjchem-1596	23	13	of	of	ADP
eurjchem-1596	23	14	intercourse	intercourse	NOUN
eurjchem-1596	23	15	,	,	PUNCT
eurjchem-1596	23	16	that	that	PRON
eurjchem-1596	23	17	extending	extend	VERB
eurjchem-1596	23	18	the	the	DET
eurjchem-1596	23	19	window	window	NOUN
eurjchem-1596	23	20	of	of	ADP
eurjchem-1596	23	21	oppor‐	oppor‐	NOUN
eurjchem-1596	23	22	tunity	tunity	NOUN
eurjchem-1596	23	23	for	for	ADP
eurjchem-1596	23	24	ec	ec	PROPN
eurjchem-1596	24	1	[	[	X
eurjchem-1596	24	2	3	3	NUM
eurjchem-1596	24	3	]	]	PUNCT
eurjchem-1596	24	4	.	.	PUNCT
eurjchem-1596	25	1	it	it	PRON
eurjchem-1596	25	2	prevents	prevent	VERB
eurjchem-1596	25	3	progesterone	progesterone	NOUN
eurjchem-1596	25	4	from	from	ADP
eurjchem-1596	25	5	binding	bind	VERB
eurjchem-1596	25	6	to	to	ADP
eurjchem-1596	25	7	its	its	PRON
eurjchem-1596	25	8	receptor	receptor	NOUN
eurjchem-1596	25	9	,	,	PUNCT
eurjchem-1596	25	10	therefore	therefore	ADV
eurjchem-1596	25	11	the	the	DET
eurjchem-1596	25	12	gene	gene	NOUN
eurjchem-1596	25	13	transcription	transcription	NOUN
eurjchem-1596	25	14	normally	normally	ADV
eurjchem-1596	25	15	turned	turn	VERB
eurjchem-1596	25	16	on	on	ADP
eurjchem-1596	25	17	by	by	ADP
eurjchem-1596	25	18	progesterone	progesterone	NOUN
eurjchem-1596	25	19	was	be	AUX
eurjchem-1596	25	20	blocked	block	VERB
eurjchem-1596	25	21	,	,	PUNCT
eurjchem-1596	25	22	and	and	CCONJ
eurjchem-1596	25	23	the	the	DET
eurjchem-1596	25	24	proteins	protein	NOUN
eurjchem-1596	25	25	necessary	necessary	ADJ
eurjchem-1596	25	26	to	to	PART
eurjchem-1596	25	27	begin	begin	VERB
eurjchem-1596	25	28	and	and	CCONJ
eurjchem-1596	25	29	maintain	maintain	VERB
eurjchem-1596	25	30	pregnancy	pregnancy	NOUN
eurjchem-1596	25	31	are	be	AUX
eurjchem-1596	25	32	not	not	PART
eurjchem-1596	25	33	synthesized	synthesize	VERB
eurjchem-1596	25	34	[	[	PUNCT
eurjchem-1596	25	35	4	4	NUM
eurjchem-1596	25	36	]	]	PUNCT
eurjchem-1596	25	37	.	.	PUNCT
eurjchem-1596	26	1	ulipristal	ulipristal	ADJ
eurjchem-1596	26	2	acetate	acetate	PROPN
eurjchem-1596	26	3	5	5	NUM
eurjchem-1596	26	4	mg	mg	PROPN
eurjchem-1596	26	5	dose	dose	NOUN
eurjchem-1596	26	6	is	be	AUX
eurjchem-1596	26	7	also	also	ADV
eurjchem-1596	26	8	used	use	VERB
eurjchem-1596	26	9	for	for	ADP
eurjchem-1596	26	10	the	the	DET
eurjchem-1596	26	11	treatment	treatment	NOUN
eurjchem-1596	26	12	of	of	ADP
eurjchem-1596	26	13	uterine	uterine	ADJ
eurjchem-1596	26	14	fibroids	fibroid	NOUN
eurjchem-1596	26	15	due	due	ADP
eurjchem-1596	26	16	to	to	ADP
eurjchem-1596	26	17	its	its	PRON
eurjchem-1596	26	18	safety	safety	NOUN
eurjchem-1596	26	19	and	and	CCONJ
eurjchem-1596	26	20	efficacy	efficacy	NOUN
eurjchem-1596	26	21	[	[	X
eurjchem-1596	26	22	5	5	NUM
eurjchem-1596	26	23	]	]	PUNCT
eurjchem-1596	26	24	.	.	PUNCT
eurjchem-1596	27	1	following	follow	VERB
eurjchem-1596	27	2	oral	oral	ADJ
eurjchem-1596	27	3	administration	administration	NOUN
eurjchem-1596	27	4	ulipristal	ulipristal	PROPN
eurjchem-1596	27	5	acetate	acetate	PROPN
eurjchem-1596	27	6	rapidly	rapidly	ADV
eurjchem-1596	27	7	absorbed	absorb	VERB
eurjchem-1596	27	8	with	with	ADP
eurjchem-1596	27	9	peak	peak	NOUN
eurjchem-1596	27	10	plasma	plasma	NOUN
eurjchem-1596	27	11	concentration	concentration	NOUN
eurjchem-1596	27	12	of	of	ADP
eurjchem-1596	27	13	176±89	176±89	PROPN
eurjchem-1596	27	14	ng	ng	PROPN
eurjchem-1596	27	15	/	/	SYM
eurjchem-1596	27	16	ml	ml	PROPN
eurjchem-1596	27	17	,	,	PUNCT
eurjchem-1596	27	18	and	and	CCONJ
eurjchem-1596	27	19	was	be	AUX
eurjchem-1596	27	20	extensively	extensively	ADV
eurjchem-1596	27	21	metabolized	metabolize	VERB
eurjchem-1596	27	22	by	by	ADP
eurjchem-1596	27	23	cyp3a4	cyp3a4	NOUN
eurjchem-1596	27	24	in	in	ADP
eurjchem-1596	27	25	liver	liver	NOUN
eurjchem-1596	27	26	and	and	CCONJ
eurjchem-1596	27	27	the	the	DET
eurjchem-1596	27	28	principal	principal	ADJ
eurjchem-1596	27	29	metabolites	metabolite	NOUN
eurjchem-1596	27	30	formed	form	VERB
eurjchem-1596	27	31	are	be	AUX
eurjchem-1596	27	32	mono	mono	NOUN
eurjchem-1596	27	33	and	and	CCONJ
eurjchem-1596	27	34	di	di	NOUN
eurjchem-1596	27	35	demethylated	demethylate	VERB
eurjchem-1596	27	36	derivatives	derivative	NOUN
eurjchem-1596	27	37	,	,	PUNCT
eurjchem-1596	27	38	of	of	ADP
eurjchem-1596	27	39	which	which	PRON
eurjchem-1596	27	40	mono	mono	NOUN
eurjchem-1596	27	41	demethylated	demethylate	VERB
eurjchem-1596	27	42	derivative	derivative	NOUN
eurjchem-1596	27	43	was	be	AUX
eurjchem-1596	27	44	pharmacolo‐	pharmacolo‐	ADV
eurjchem-1596	27	45	gically	gically	ADV
eurjchem-1596	27	46	active	active	ADJ
eurjchem-1596	27	47	[	[	X
eurjchem-1596	27	48	6	6	NUM
eurjchem-1596	27	49	]	]	PUNCT
eurjchem-1596	27	50	.	.	PUNCT
eurjchem-1596	28	1	the	the	DET
eurjchem-1596	28	2	measurement	measurement	NOUN
eurjchem-1596	28	3	of	of	ADP
eurjchem-1596	28	4	ulipristal	ulipristal	ADJ
eurjchem-1596	28	5	acetate	acetate	NOUN
eurjchem-1596	28	6	itself	itself	PRON
eurjchem-1596	28	7	would	would	AUX
eurjchem-1596	28	8	suffice	suffice	VERB
eurjchem-1596	28	9	for	for	ADP
eurjchem-1596	28	10	bioequivalence	bioequivalence	NOUN
eurjchem-1596	28	11	and	and	CCONJ
eurjchem-1596	28	12	pharmacokinetic	pharmacokinetic	ADJ
eurjchem-1596	28	13	studies	study	NOUN
eurjchem-1596	28	14	that	that	PRON
eurjchem-1596	28	15	support	support	VERB
eurjchem-1596	28	16	for	for	ADP
eurjchem-1596	28	17	regulatory	regulatory	ADJ
eurjchem-1596	28	18	submissions	submission	NOUN
eurjchem-1596	28	19	in	in	ADP
eurjchem-1596	28	20	commercial	commercial	ADJ
eurjchem-1596	28	21	envi‐	envi‐	VERB
eurjchem-1596	28	22	ronment	ronment	ADJ
eurjchem-1596	28	23	.	.	PUNCT
eurjchem-1596	29	1	in	in	ADP
eurjchem-1596	29	2	literature	literature	NOUN
eurjchem-1596	29	3	hplc	hplc	NOUN
eurjchem-1596	29	4	method	method	NOUN
eurjchem-1596	29	5	was	be	AUX
eurjchem-1596	29	6	reported	report	VERB
eurjchem-1596	29	7	[	[	X
eurjchem-1596	29	8	7	7	NUM
eurjchem-1596	29	9	]	]	PUNCT
eurjchem-1596	29	10	and	and	CCONJ
eurjchem-1596	29	11	lc‐	lc‐	ADJ
eurjchem-1596	29	12	ms	ms	PROPN
eurjchem-1596	29	13	/	/	SYM
eurjchem-1596	29	14	ms	ms	PROPN
eurjchem-1596	29	15	methods	method	NOUN
eurjchem-1596	29	16	used	use	VERB
eurjchem-1596	29	17	in	in	ADP
eurjchem-1596	29	18	some	some	DET
eurjchem-1596	29	19	clinical	clinical	ADJ
eurjchem-1596	29	20	trials	trial	NOUN
eurjchem-1596	29	21	were	be	AUX
eurjchem-1596	29	22	reported	report	VERB
eurjchem-1596	29	23	for	for	ADP
eurjchem-1596	29	24	determination	determination	NOUN
eurjchem-1596	29	25	of	of	ADP
eurjchem-1596	29	26	ulipristal	ulipristal	ADJ
eurjchem-1596	29	27	acetate	acetate	NOUN
eurjchem-1596	30	1	[	[	X
eurjchem-1596	30	2	5,8	5,8	NUM
eurjchem-1596	30	3	]	]	PUNCT
eurjchem-1596	30	4	,	,	PUNCT
eurjchem-1596	30	5	to	to	ADP
eurjchem-1596	30	6	the	the	DET
eurjchem-1596	30	7	best	good	ADJ
eurjchem-1596	30	8	of	of	ADP
eurjchem-1596	30	9	our	our	PRON
eurjchem-1596	30	10	knowledge	knowledge	NOUN
eurjchem-1596	30	11	no	no	DET
eurjchem-1596	30	12	specific	specific	ADJ
eurjchem-1596	30	13	lc‐ms	lc‐ms	AUX
eurjchem-1596	30	14	/	/	SYM
eurjchem-1596	30	15	ms	ms	PROPN
eurjchem-1596	30	16	method	method	NOUN
eurjchem-1596	30	17	was	be	AUX
eurjchem-1596	30	18	published	publish	VERB
eurjchem-1596	30	19	till	till	SCONJ
eurjchem-1596	30	20	today	today	NOUN
eurjchem-1596	30	21	for	for	ADP
eurjchem-1596	30	22	analysis	analysis	NOUN
eurjchem-1596	30	23	of	of	ADP
eurjchem-1596	30	24	ulipristal	ulipristal	ADJ
eurjchem-1596	30	25	acetate	acetate	NOUN
eurjchem-1596	30	26	in	in	ADP
eurjchem-1596	30	27	human	human	ADJ
eurjchem-1596	30	28	plasma	plasma	NOUN
eurjchem-1596	30	29	.	.	PUNCT
eurjchem-1596	31	1	in	in	ADP
eurjchem-1596	31	2	present	present	ADJ
eurjchem-1596	31	3	study	study	NOUN
eurjchem-1596	31	4	,	,	PUNCT
eurjchem-1596	31	5	optimized	optimize	VERB
eurjchem-1596	31	6	chromatographic	chromatographic	ADJ
eurjchem-1596	31	7	conditions	condition	NOUN
eurjchem-1596	31	8	were	be	AUX
eurjchem-1596	31	9	developed	develop	VERB
eurjchem-1596	31	10	for	for	ADP
eurjchem-1596	31	11	the	the	DET
eurjchem-1596	31	12	analysis	analysis	NOUN
eurjchem-1596	31	13	of	of	ADP
eurjchem-1596	31	14	ulipristal	ulipristal	ADJ
eurjchem-1596	31	15	acetate	acetate	NOUN
eurjchem-1596	31	16	in	in	ADP
eurjchem-1596	31	17	plasma	plasma	NOUN
eurjchem-1596	31	18	samples	sample	NOUN
eurjchem-1596	31	19	.	.	PUNCT
eurjchem-1596	32	1	the	the	DET
eurjchem-1596	32	2	lloq	lloq	NOUN
eurjchem-1596	32	3	achieved	achieve	VERB
eurjchem-1596	32	4	is	be	AUX
eurjchem-1596	32	5	1	1	NUM
eurjchem-1596	32	6	ng	ng	PROPN
eurjchem-1596	32	7	/	/	SYM
eurjchem-1596	32	8	ml	ml	PROPN
eurjchem-1596	32	9	and	and	CCONJ
eurjchem-1596	32	10	chromatographic	chromatographic	ADJ
eurjchem-1596	32	11	runtime	runtime	NOUN
eurjchem-1596	32	12	was	be	AUX
eurjchem-1596	32	13	2	2	NUM
eurjchem-1596	32	14	min	min	NOUN
eurjchem-1596	32	15	.	.	PROPN
eurjchem-1596	32	16	pappula	pappula	PROPN
eurjchem-1596	32	17	et	et	PROPN
eurjchem-1596	32	18	al	al	PROPN
eurjchem-1596	32	19	.	.	PUNCT
eurjchem-1596	32	20	/	/	SYM
eurjchem-1596	32	21	european	european	PROPN
eurjchem-1596	32	22	journal	journal	PROPN
eurjchem-1596	32	23	of	of	ADP
eurjchem-1596	32	24	chemistry	chemistry	NOUN
eurjchem-1596	32	25	8	8	NUM
eurjchem-1596	32	26	(	(	PUNCT
eurjchem-1596	32	27	3	3	NUM
eurjchem-1596	32	28	)	)	PUNCT
eurjchem-1596	32	29	(	(	PUNCT
eurjchem-1596	32	30	2017	2017	NUM
eurjchem-1596	32	31	)	)	PUNCT
eurjchem-1596	32	32	258‐264	258‐264	NOUN
eurjchem-1596	32	33	259	259	NUM
eurjchem-1596	32	34	(	(	PUNCT
eurjchem-1596	32	35	a	a	NOUN
eurjchem-1596	32	36	)	)	PUNCT
eurjchem-1596	32	37	(	(	PUNCT
eurjchem-1596	32	38	b	b	X
eurjchem-1596	32	39	)	)	PUNCT
eurjchem-1596	32	40	figure	figure	NOUN
eurjchem-1596	32	41	1	1	NUM
eurjchem-1596	32	42	.	.	PUNCT
eurjchem-1596	32	43	product	product	NOUN
eurjchem-1596	32	44	ion	ion	NOUN
eurjchem-1596	32	45	spectra	spectra	NOUN
eurjchem-1596	32	46	of	of	ADP
eurjchem-1596	32	47	(	(	PUNCT
eurjchem-1596	32	48	a	a	PRON
eurjchem-1596	32	49	)	)	PUNCT
eurjchem-1596	32	50	ulipristal	ulipristal	ADJ
eurjchem-1596	32	51	acetate	acetate	NOUN
eurjchem-1596	32	52	(	(	PUNCT
eurjchem-1596	32	53	m	m	NOUN
eurjchem-1596	32	54	/	/	SYM
eurjchem-1596	32	55	z	z	NOUN
eurjchem-1596	32	56	=	=	SYM
eurjchem-1596	32	57	476.2/134.1	476.2/134.1	NUM
eurjchem-1596	32	58	)	)	PUNCT
eurjchem-1596	32	59	and	and	CCONJ
eurjchem-1596	32	60	(	(	PUNCT
eurjchem-1596	32	61	b	b	NOUN
eurjchem-1596	32	62	)	)	PUNCT
eurjchem-1596	32	63	levonorgestrel	levonorgestrel	NOUN
eurjchem-1596	32	64	(	(	PUNCT
eurjchem-1596	32	65	m	m	NOUN
eurjchem-1596	32	66	/	/	SYM
eurjchem-1596	32	67	z	z	NOUN
eurjchem-1596	32	68	=	=	SYM
eurjchem-1596	32	69	313.3/245.1	313.3/245.1	NUM
eurjchem-1596	32	70	)	)	PUNCT
eurjchem-1596	32	71	.	.	PUNCT
eurjchem-1596	33	1	2	2	X
eurjchem-1596	33	2	.	.	X
eurjchem-1596	33	3	experimental	experimental	ADJ
eurjchem-1596	33	4	2.1	2.1	NUM
eurjchem-1596	33	5	.	.	PUNCT
eurjchem-1596	33	6	materials	material	NOUN
eurjchem-1596	33	7	and	and	CCONJ
eurjchem-1596	33	8	reagents	reagent	NOUN
eurjchem-1596	33	9	the	the	DET
eurjchem-1596	33	10	ulipristal	ulipristal	ADJ
eurjchem-1596	33	11	acetate	acetate	PROPN
eurjchem-1596	33	12	reference	reference	PROPN
eurjchem-1596	33	13	standard	standard	PROPN
eurjchem-1596	33	14	and	and	CCONJ
eurjchem-1596	33	15	internal	internal	ADJ
eurjchem-1596	33	16	standard	standard	NOUN
eurjchem-1596	33	17	(	(	PUNCT
eurjchem-1596	33	18	istd	istd	NOUN
eurjchem-1596	33	19	;	;	PUNCT
eurjchem-1596	33	20	levonorgestrel	levonorgestrel	NOUN
eurjchem-1596	33	21	)	)	PUNCT
eurjchem-1596	33	22	were	be	AUX
eurjchem-1596	33	23	obtained	obtain	VERB
eurjchem-1596	33	24	from	from	ADP
eurjchem-1596	33	25	clear‐	clear‐	NOUN
eurjchem-1596	33	26	synth	synth	NOUN
eurjchem-1596	33	27	labs	lab	NOUN
eurjchem-1596	33	28	.	.	PUNCT
eurjchem-1596	34	1	mumbai	mumbai	PROPN
eurjchem-1596	34	2	,	,	PUNCT
eurjchem-1596	34	3	india	india	PROPN
eurjchem-1596	34	4	.	.	PUNCT
eurjchem-1596	35	1	gradient	gradient	ADJ
eurjchem-1596	35	2	grade	grade	NOUN
eurjchem-1596	35	3	lichro‐solv	lichro‐solv	NOUN
eurjchem-1596	35	4	methanol	methanol	NOUN
eurjchem-1596	35	5	,	,	PUNCT
eurjchem-1596	35	6	acetonitrile	acetonitrile	NOUN
eurjchem-1596	35	7	(	(	PUNCT
eurjchem-1596	35	8	acn	acn	PROPN
eurjchem-1596	35	9	)	)	PUNCT
eurjchem-1596	35	10	,	,	PUNCT
eurjchem-1596	35	11	analytical	analytical	ADJ
eurjchem-1596	35	12	grade	grade	NOUN
eurjchem-1596	35	13	ammonium	ammonium	NOUN
eurjchem-1596	35	14	formate	formate	NOUN
eurjchem-1596	35	15	,	,	PUNCT
eurjchem-1596	35	16	sodium	sodium	NOUN
eurjchem-1596	35	17	carbonate	carbonate	NOUN
eurjchem-1596	35	18	and	and	CCONJ
eurjchem-1596	35	19	formic	formic	ADJ
eurjchem-1596	35	20	acid	acid	NOUN
eurjchem-1596	35	21	(	(	PUNCT
eurjchem-1596	35	22	gr	gr	NOUN
eurjchem-1596	35	23	grade	grade	NOUN
eurjchem-1596	35	24	)	)	PUNCT
eurjchem-1596	35	25	were	be	AUX
eurjchem-1596	35	26	purchased	purchase	VERB
eurjchem-1596	35	27	from	from	ADP
eurjchem-1596	35	28	merck	merck	PROPN
eurjchem-1596	35	29	specialities	speciality	NOUN
eurjchem-1596	35	30	(	(	PUNCT
eurjchem-1596	35	31	mumbai	mumbai	PROPN
eurjchem-1596	35	32	,	,	PUNCT
eurjchem-1596	35	33	india	india	PROPN
eurjchem-1596	35	34	)	)	PUNCT
eurjchem-1596	35	35	.	.	PUNCT
eurjchem-1596	36	1	methyl	methyl	NOUN
eurjchem-1596	36	2	tert‐butyl	tert‐butyl	ADP
eurjchem-1596	36	3	ether	ether	NOUN
eurjchem-1596	36	4	and	and	CCONJ
eurjchem-1596	36	5	n‐hexane	n‐hexane	NUM
eurjchem-1596	36	6	were	be	AUX
eurjchem-1596	36	7	purchased	purchase	VERB
eurjchem-1596	36	8	from	from	ADP
eurjchem-1596	36	9	rankem	rankem	PROPN
eurjchem-1596	36	10	(	(	PUNCT
eurjchem-1596	36	11	mumbai	mumbai	PROPN
eurjchem-1596	36	12	,	,	PUNCT
eurjchem-1596	36	13	india	india	PROPN
eurjchem-1596	36	14	)	)	PUNCT
eurjchem-1596	36	15	.	.	PUNCT
eurjchem-1596	37	1	ultrapure	ultrapure	NOUN
eurjchem-1596	37	2	type‐1	type‐1	NOUN
eurjchem-1596	37	3	water	water	NOUN
eurjchem-1596	37	4	from	from	ADP
eurjchem-1596	37	5	milli‐q	milli‐q	NOUN
eurjchem-1596	37	6	system	system	NOUN
eurjchem-1596	37	7	(	(	PUNCT
eurjchem-1596	37	8	millipore	millipore	PROPN
eurjchem-1596	37	9	,	,	PUNCT
eurjchem-1596	37	10	bedford	bedford	PROPN
eurjchem-1596	37	11	,	,	PUNCT
eurjchem-1596	37	12	ma	ma	PROPN
eurjchem-1596	37	13	,	,	PUNCT
eurjchem-1596	37	14	usa	usa	PROPN
eurjchem-1596	37	15	)	)	PUNCT
eurjchem-1596	37	16	was	be	AUX
eurjchem-1596	37	17	used	use	VERB
eurjchem-1596	37	18	for	for	ADP
eurjchem-1596	37	19	all	all	DET
eurjchem-1596	37	20	preparations	preparation	NOUN
eurjchem-1596	37	21	in	in	ADP
eurjchem-1596	37	22	the	the	DET
eurjchem-1596	37	23	study	study	NOUN
eurjchem-1596	37	24	.	.	PUNCT
eurjchem-1596	38	1	polypropylene	polypropylene	PROPN
eurjchem-1596	38	2	ria	ria	PROPN
eurjchem-1596	38	3	vials	vial	NOUN
eurjchem-1596	38	4	(	(	PUNCT
eurjchem-1596	38	5	abdos	abdo	VERB
eurjchem-1596	38	6	,	,	PUNCT
eurjchem-1596	38	7	new	new	ADJ
eurjchem-1596	38	8	delhi	delhi	PROPN
eurjchem-1596	38	9	,	,	PUNCT
eurjchem-1596	38	10	india	india	PROPN
eurjchem-1596	38	11	)	)	PUNCT
eurjchem-1596	38	12	and	and	CCONJ
eurjchem-1596	38	13	volumetric	volumetric	NOUN
eurjchem-1596	38	14	flasks	flask	NOUN
eurjchem-1596	38	15	(	(	PUNCT
eurjchem-1596	38	16	type	type	NOUN
eurjchem-1596	38	17	a	a	PRON
eurjchem-1596	38	18	)	)	PUNCT
eurjchem-1596	38	19	were	be	AUX
eurjchem-1596	38	20	obtained	obtain	VERB
eurjchem-1596	38	21	from	from	ADP
eurjchem-1596	38	22	tarsons	tarson	NOUN
eurjchem-1596	38	23	products	products	PROPN
eurjchem-1596	38	24	pvt	pvt	PROPN
eurjchem-1596	38	25	.	.	PROPN
eurjchem-1596	38	26	ltd	ltd	PROPN
eurjchem-1596	38	27	.	.	PUNCT
eurjchem-1596	39	1	new	new	PROPN
eurjchem-1596	39	2	delhi	delhi	PROPN
eurjchem-1596	39	3	,	,	PUNCT
eurjchem-1596	39	4	india	india	PROPN
eurjchem-1596	39	5	.	.	PUNCT
eurjchem-1596	40	1	a	a	DET
eurjchem-1596	40	2	liquid‐liquid	liquid‐liquid	ADJ
eurjchem-1596	40	3	extraction	extraction	NOUN
eurjchem-1596	40	4	vwr	vwr	PROPN
eurjchem-1596	40	5	multi	multi	PROPN
eurjchem-1596	40	6	tube	tube	PROPN
eurjchem-1596	40	7	vortexer	vortexer	NOUN
eurjchem-1596	40	8	(	(	PUNCT
eurjchem-1596	40	9	bangalore	bangalore	PROPN
eurjchem-1596	40	10	,	,	PUNCT
eurjchem-1596	40	11	india	india	PROPN
eurjchem-1596	40	12	)	)	PUNCT
eurjchem-1596	40	13	was	be	AUX
eurjchem-1596	40	14	used	use	VERB
eurjchem-1596	40	15	for	for	ADP
eurjchem-1596	40	16	preparation	preparation	NOUN
eurjchem-1596	40	17	of	of	ADP
eurjchem-1596	40	18	samples	sample	NOUN
eurjchem-1596	40	19	.	.	PUNCT
eurjchem-1596	41	1	2.2	2.2	NUM
eurjchem-1596	41	2	.	.	PUNCT
eurjchem-1596	41	3	mass	mass	ADJ
eurjchem-1596	41	4	spectroscopic	spectroscopic	ADJ
eurjchem-1596	41	5	and	and	CCONJ
eurjchem-1596	41	6	chromatographic	chromatographic	ADJ
eurjchem-1596	41	7	conditions	condition	NOUN
eurjchem-1596	41	8	the	the	DET
eurjchem-1596	41	9	hplc	hplc	NOUN
eurjchem-1596	41	10	sil	sil	PROPN
eurjchem-1596	41	11	htc	htc	NOUN
eurjchem-1596	41	12	system	system	NOUN
eurjchem-1596	41	13	(	(	PUNCT
eurjchem-1596	41	14	shimadzu	shimadzu	PROPN
eurjchem-1596	41	15	corporation	corporation	NOUN
eurjchem-1596	41	16	,	,	PUNCT
eurjchem-1596	41	17	kyoto	kyoto	PROPN
eurjchem-1596	41	18	,	,	PUNCT
eurjchem-1596	41	19	japan	japan	PROPN
eurjchem-1596	41	20	)	)	PUNCT
eurjchem-1596	41	21	is	be	AUX
eurjchem-1596	41	22	equipped	equip	VERB
eurjchem-1596	41	23	with	with	ADP
eurjchem-1596	41	24	an	an	DET
eurjchem-1596	41	25	lc‐ad	lc‐ad	NUM
eurjchem-1596	41	26	vp	vp	PROPN
eurjchem-1596	41	27	binary	binary	PROPN
eurjchem-1596	41	28	pump	pump	PROPN
eurjchem-1596	41	29	,	,	PUNCT
eurjchem-1596	41	30	a	a	DET
eurjchem-1596	41	31	dgu20a5	dgu20a5	PROPN
eurjchem-1596	41	32	degasser	degasser	PROPN
eurjchem-1596	41	33	,	,	PUNCT
eurjchem-1596	41	34	and	and	CCONJ
eurjchem-1596	41	35	a	a	DET
eurjchem-1596	41	36	sil‐htc	sil‐htc	ADJ
eurjchem-1596	41	37	auto	auto	NOUN
eurjchem-1596	41	38	sampler	sampler	NOUN
eurjchem-1596	41	39	with	with	ADP
eurjchem-1596	41	40	a	a	DET
eurjchem-1596	41	41	cto‐10as	cto‐10as	ADV
eurjchem-1596	41	42	vp	vp	NOUN
eurjchem-1596	41	43	thermostat	thermostat	NOUN
eurjchem-1596	41	44	column	column	NOUN
eurjchem-1596	41	45	oven	oven	VERB
eurjchem-1596	41	46	maintained	maintain	VERB
eurjchem-1596	41	47	at	at	ADP
eurjchem-1596	41	48	35	35	NUM
eurjchem-1596	41	49	°	°	NOUN
eurjchem-1596	41	50	c	c	NOUN
eurjchem-1596	41	51	temperature	temperature	NOUN
eurjchem-1596	41	52	.	.	PUNCT
eurjchem-1596	42	1	kinetex	kinetex	NOUN
eurjchem-1596	42	2	5	5	NUM
eurjchem-1596	42	3	µm	µm	ADP
eurjchem-1596	42	4	evo	evo	PROPN
eurjchem-1596	42	5	c18	c18	PROPN
eurjchem-1596	42	6	,	,	PUNCT
eurjchem-1596	42	7	column	column	NOUN
eurjchem-1596	42	8	(	(	PUNCT
eurjchem-1596	42	9	50	50	NUM
eurjchem-1596	42	10	mm	mm	NOUN
eurjchem-1596	42	11	in	in	ADP
eurjchem-1596	42	12	length	length	NOUN
eurjchem-1596	42	13	,	,	PUNCT
eurjchem-1596	42	14	4.6	4.6	NUM
eurjchem-1596	42	15	mm	mm	NOUN
eurjchem-1596	42	16	internal	internal	ADJ
eurjchem-1596	42	17	diameter	diameter	NOUN
eurjchem-1596	42	18	,	,	PUNCT
eurjchem-1596	42	19	and	and	CCONJ
eurjchem-1596	42	20	5	5	NUM
eurjchem-1596	42	21	µ	µ	PRON
eurjchem-1596	42	22	particle	particle	NOUN
eurjchem-1596	42	23	size	size	NOUN
eurjchem-1596	42	24	)	)	PUNCT
eurjchem-1596	42	25	was	be	AUX
eurjchem-1596	42	26	used	use	VERB
eurjchem-1596	42	27	as	as	ADP
eurjchem-1596	42	28	stationary	stationary	ADJ
eurjchem-1596	42	29	phase	phase	NOUN
eurjchem-1596	42	30	.	.	PUNCT
eurjchem-1596	43	1	the	the	DET
eurjchem-1596	43	2	analyte	analyte	NOUN
eurjchem-1596	43	3	and	and	CCONJ
eurjchem-1596	43	4	internal	internal	ADJ
eurjchem-1596	43	5	standard	standard	NOUN
eurjchem-1596	43	6	were	be	AUX
eurjchem-1596	43	7	chromate‐	chromate‐	NOUN
eurjchem-1596	43	8	graphed	graph	VERB
eurjchem-1596	43	9	isocratically	isocratically	ADV
eurjchem-1596	43	10	using	use	VERB
eurjchem-1596	43	11	mobile	mobile	ADJ
eurjchem-1596	43	12	phase	phase	NOUN
eurjchem-1596	43	13	consisting	consist	VERB
eurjchem-1596	43	14	of	of	ADP
eurjchem-1596	43	15	a	a	DET
eurjchem-1596	43	16	mixture	mixture	NOUN
eurjchem-1596	43	17	of	of	ADP
eurjchem-1596	43	18	10	10	NUM
eurjchem-1596	43	19	mm	mm	NOUN
eurjchem-1596	43	20	ammonium	ammonium	NOUN
eurjchem-1596	43	21	formate	formate	NOUN
eurjchem-1596	43	22	ph	ph	NOUN
eurjchem-1596	43	23	=	=	SYM
eurjchem-1596	43	24	3.5	3.5	NUM
eurjchem-1596	43	25	(	(	PUNCT
eurjchem-1596	43	26	adjusted	adjust	VERB
eurjchem-1596	43	27	with	with	ADP
eurjchem-1596	43	28	formic	formic	ADJ
eurjchem-1596	43	29	acid	acid	NOUN
eurjchem-1596	43	30	)	)	PUNCT
eurjchem-1596	43	31	,	,	PUNCT
eurjchem-1596	43	32	and	and	CCONJ
eurjchem-1596	43	33	acetonitrile	acetonitrile	NOUN
eurjchem-1596	43	34	(	(	PUNCT
eurjchem-1596	43	35	10:90	10:90	NUM
eurjchem-1596	43	36	,	,	PUNCT
eurjchem-1596	43	37	v	v	NOUN
eurjchem-1596	43	38	:	:	PUNCT
eurjchem-1596	43	39	v	v	NOUN
eurjchem-1596	43	40	)	)	PUNCT
eurjchem-1596	43	41	.	.	PUNCT
eurjchem-1596	44	1	the	the	DET
eurjchem-1596	44	2	flow	flow	NOUN
eurjchem-1596	44	3	rate	rate	NOUN
eurjchem-1596	44	4	was	be	AUX
eurjchem-1596	44	5	set	set	VERB
eurjchem-1596	44	6	at	at	ADP
eurjchem-1596	44	7	0.6	0.6	NUM
eurjchem-1596	44	8	ml	ml	NOUN
eurjchem-1596	44	9	/	/	SYM
eurjchem-1596	44	10	min	min	NOUN
eurjchem-1596	44	11	.	.	PUNCT
eurjchem-1596	45	1	the	the	DET
eurjchem-1596	45	2	mobile	mobile	ADJ
eurjchem-1596	45	3	phase	phase	NOUN
eurjchem-1596	45	4	flow	flow	NOUN
eurjchem-1596	45	5	was	be	AUX
eurjchem-1596	45	6	controlled	control	VERB
eurjchem-1596	45	7	by	by	ADP
eurjchem-1596	45	8	using	use	VERB
eurjchem-1596	45	9	split	split	NOUN
eurjchem-1596	45	10	,	,	PUNCT
eurjchem-1596	45	11	so	so	SCONJ
eurjchem-1596	45	12	that	that	SCONJ
eurjchem-1596	45	13	50	50	NUM
eurjchem-1596	45	14	%	%	NOUN
eurjchem-1596	45	15	of	of	ADP
eurjchem-1596	45	16	total	total	ADJ
eurjchem-1596	45	17	flow	flow	NOUN
eurjchem-1596	45	18	was	be	AUX
eurjchem-1596	45	19	injected	inject	VERB
eurjchem-1596	45	20	to	to	ADP
eurjchem-1596	45	21	the	the	DET
eurjchem-1596	45	22	ms	ms	PROPN
eurjchem-1596	45	23	system	system	NOUN
eurjchem-1596	45	24	.	.	PUNCT
eurjchem-1596	46	1	mass	mass	PROPN
eurjchem-1596	46	2	spectrometric	spectrometric	ADJ
eurjchem-1596	46	3	detection	detection	NOUN
eurjchem-1596	46	4	performed	perform	VERB
eurjchem-1596	46	5	using	use	VERB
eurjchem-1596	46	6	api	api	NOUN
eurjchem-1596	46	7	4000	4000	NUM
eurjchem-1596	46	8	triple	triple	ADJ
eurjchem-1596	46	9	quadrupole	quadrupole	NOUN
eurjchem-1596	46	10	instrument	instrument	NOUN
eurjchem-1596	46	11	(	(	PUNCT
eurjchem-1596	46	12	mds‐sciex	mds‐sciex	ADV
eurjchem-1596	46	13	,	,	PUNCT
eurjchem-1596	46	14	concord	concord	PROPN
eurjchem-1596	46	15	,	,	PUNCT
eurjchem-1596	46	16	ontario	ontario	PROPN
eurjchem-1596	46	17	,	,	PUNCT
eurjchem-1596	46	18	canada	canada	PROPN
eurjchem-1596	46	19	)	)	PUNCT
eurjchem-1596	46	20	operated	operate	VERB
eurjchem-1596	46	21	in	in	ADP
eurjchem-1596	46	22	a	a	DET
eurjchem-1596	46	23	multiple	multiple	ADJ
eurjchem-1596	46	24	reaction	reaction	NOUN
eurjchem-1596	46	25	mode	mode	NOUN
eurjchem-1596	46	26	(	(	PUNCT
eurjchem-1596	46	27	mrm	mrm	PROPN
eurjchem-1596	46	28	)	)	PUNCT
eurjchem-1596	46	29	.	.	PUNCT
eurjchem-1596	47	1	source	source	NOUN
eurjchem-1596	47	2	equipped	equip	VERB
eurjchem-1596	47	3	with	with	ADP
eurjchem-1596	47	4	turbo	turbo	NOUN
eurjchem-1596	47	5	ion	ion	NOUN
eurjchem-1596	47	6	spray	spray	NOUN
eurjchem-1596	47	7	in	in	ADP
eurjchem-1596	47	8	positive	positive	ADJ
eurjchem-1596	47	9	ionization	ionization	NOUN
eurjchem-1596	47	10	mode	mode	NOUN
eurjchem-1596	47	11	,	,	PUNCT
eurjchem-1596	47	12	nitrogen	nitrogen	NOUN
eurjchem-1596	47	13	gas	gas	NOUN
eurjchem-1596	47	14	used	use	VERB
eurjchem-1596	47	15	as	as	ADP
eurjchem-1596	47	16	nebulization	nebulization	NOUN
eurjchem-1596	47	17	gas	gas	NOUN
eurjchem-1596	47	18	(	(	PUNCT
eurjchem-1596	47	19	gs1	gs1	NOUN
eurjchem-1596	47	20	35	35	NUM
eurjchem-1596	47	21	)	)	PUNCT
eurjchem-1596	47	22	and	and	CCONJ
eurjchem-1596	47	23	heater	heater	NOUN
eurjchem-1596	47	24	gas	gas	NOUN
eurjchem-1596	47	25	(	(	PUNCT
eurjchem-1596	47	26	gs2	gs2	PROPN
eurjchem-1596	47	27	35	35	NUM
eurjchem-1596	47	28	)	)	PUNCT
eurjchem-1596	47	29	for	for	ADP
eurjchem-1596	47	30	desolvation	desolvation	NOUN
eurjchem-1596	47	31	,	,	PUNCT
eurjchem-1596	47	32	source	source	NOUN
eurjchem-1596	47	33	temperature	temperature	NOUN
eurjchem-1596	47	34	was	be	AUX
eurjchem-1596	47	35	maintained	maintain	VERB
eurjchem-1596	47	36	at	at	ADP
eurjchem-1596	47	37	500	500	NUM
eurjchem-1596	47	38	°	°	NOUN
eurjchem-1596	47	39	c	c	NOUN
eurjchem-1596	47	40	for	for	ADP
eurjchem-1596	47	41	solvent	solvent	ADJ
eurjchem-1596	47	42	evaporation	evaporation	NOUN
eurjchem-1596	47	43	.	.	PUNCT
eurjchem-1596	48	1	the	the	DET
eurjchem-1596	48	2	ion	ion	NOUN
eurjchem-1596	48	3	spray	spray	NOUN
eurjchem-1596	48	4	needle	needle	NOUN
eurjchem-1596	48	5	voltage	voltage	NOUN
eurjchem-1596	48	6	at	at	ADP
eurjchem-1596	48	7	5000	5000	NUM
eurjchem-1596	48	8	v	v	NOUN
eurjchem-1596	48	9	,	,	PUNCT
eurjchem-1596	48	10	entrance	entrance	NOUN
eurjchem-1596	48	11	potential	potential	NOUN
eurjchem-1596	48	12	at	at	ADP
eurjchem-1596	48	13	10	10	NUM
eurjchem-1596	48	14	v	v	NOUN
eurjchem-1596	48	15	,	,	PUNCT
eurjchem-1596	48	16	collision	collision	NOUN
eurjchem-1596	48	17	cell	cell	NOUN
eurjchem-1596	48	18	exit	exit	NOUN
eurjchem-1596	48	19	potential	potential	NOUN
eurjchem-1596	48	20	at	at	ADP
eurjchem-1596	48	21	4	4	NUM
eurjchem-1596	48	22	v	v	NOUN
eurjchem-1596	48	23	,	,	PUNCT
eurjchem-1596	48	24	declustering	declustere	VERB
eurjchem-1596	48	25	potential	potential	NOUN
eurjchem-1596	48	26	at	at	ADP
eurjchem-1596	48	27	56	56	NUM
eurjchem-1596	48	28	v	v	NOUN
eurjchem-1596	48	29	and	and	CCONJ
eurjchem-1596	48	30	collision	collision	NOUN
eurjchem-1596	48	31	energy	energy	NOUN
eurjchem-1596	48	32	were	be	AUX
eurjchem-1596	48	33	set	set	VERB
eurjchem-1596	48	34	at	at	ADP
eurjchem-1596	48	35	37	37	NUM
eurjchem-1596	48	36	v	v	NOUN
eurjchem-1596	48	37	for	for	ADP
eurjchem-1596	48	38	both	both	DET
eurjchem-1596	48	39	analyte	analyte	NOUN
eurjchem-1596	48	40	and	and	CCONJ
eurjchem-1596	48	41	istd	istd	NOUN
eurjchem-1596	48	42	.	.	PUNCT
eurjchem-1596	49	1	the	the	DET
eurjchem-1596	49	2	pre‐	pre‐	NOUN
eurjchem-1596	49	3	cursor	cursor	NOUN
eurjchem-1596	49	4	/	/	SYM
eurjchem-1596	49	5	product	product	NOUN
eurjchem-1596	49	6	ion	ion	NOUN
eurjchem-1596	49	7	transitions	transition	NOUN
eurjchem-1596	49	8	in	in	ADP
eurjchem-1596	49	9	mrm	mrm	PROPN
eurjchem-1596	49	10	mode	mode	PROPN
eurjchem-1596	49	11	were	be	AUX
eurjchem-1596	49	12	m	m	PROPN
eurjchem-1596	49	13	/	/	SYM
eurjchem-1596	49	14	z	z	PROPN
eurjchem-1596	49	15	476.2	476.2	NUM
eurjchem-1596	49	16	→	→	SYM
eurjchem-1596	49	17	m	m	NOUN
eurjchem-1596	49	18	/	/	SYM
eurjchem-1596	49	19	z	z	PROPN
eurjchem-1596	49	20	134.1	134.1	NUM
eurjchem-1596	49	21	and	and	CCONJ
eurjchem-1596	49	22	m	m	PROPN
eurjchem-1596	49	23	/	/	SYM
eurjchem-1596	49	24	z	z	PROPN
eurjchem-1596	49	25	313.3	313.3	NUM
eurjchem-1596	49	26	→	→	SYM
eurjchem-1596	49	27	m	m	NOUN
eurjchem-1596	49	28	/	/	SYM
eurjchem-1596	49	29	z	z	PROPN
eurjchem-1596	49	30	245.1	245.1	NUM
eurjchem-1596	49	31	for	for	ADP
eurjchem-1596	49	32	analyte	analyte	NOUN
eurjchem-1596	49	33	and	and	CCONJ
eurjchem-1596	49	34	istd	istd	NOUN
eurjchem-1596	49	35	,	,	PUNCT
eurjchem-1596	49	36	respectively	respectively	ADV
eurjchem-1596	49	37	.	.	PUNCT
eurjchem-1596	50	1	the	the	DET
eurjchem-1596	50	2	collision	collision	NOUN
eurjchem-1596	50	3	gas	gas	NOUN
eurjchem-1596	50	4	and	and	CCONJ
eurjchem-1596	50	5	curtain	curtain	NOUN
eurjchem-1596	50	6	gas	gas	NOUN
eurjchem-1596	50	7	were	be	AUX
eurjchem-1596	50	8	set	set	VERB
eurjchem-1596	50	9	at	at	ADP
eurjchem-1596	50	10	12	12	NUM
eurjchem-1596	50	11	and	and	CCONJ
eurjchem-1596	50	12	23	23	NUM
eurjchem-1596	50	13	(	(	PUNCT
eurjchem-1596	50	14	arbitrary	arbitrary	ADJ
eurjchem-1596	50	15	units	unit	NOUN
eurjchem-1596	50	16	)	)	PUNCT
eurjchem-1596	50	17	,	,	PUNCT
eurjchem-1596	50	18	respectively	respectively	ADV
eurjchem-1596	50	19	.	.	PUNCT
eurjchem-1596	51	1	instrument	instrument	NOUN
eurjchem-1596	51	2	control	control	PROPN
eurjchem-1596	51	3	,	,	PUNCT
eurjchem-1596	51	4	data	datum	NOUN
eurjchem-1596	51	5	acquisition	acquisition	NOUN
eurjchem-1596	51	6	and	and	CCONJ
eurjchem-1596	51	7	processing	processing	NOUN
eurjchem-1596	51	8	was	be	AUX
eurjchem-1596	51	9	done	do	VERB
eurjchem-1596	51	10	with	with	ADP
eurjchem-1596	51	11	analyst	analyst	NOUN
eurjchem-1596	51	12	1.4.2	1.4.2	NUM
eurjchem-1596	51	13	software	software	NOUN
eurjchem-1596	51	14	(	(	PUNCT
eurjchem-1596	51	15	mds‐sciex	mds‐sciex	ADV
eurjchem-1596	51	16	,	,	PUNCT
eurjchem-1596	51	17	concord	concord	PROPN
eurjchem-1596	51	18	,	,	PUNCT
eurjchem-1596	51	19	ontario	ontario	PROPN
eurjchem-1596	51	20	,	,	PUNCT
eurjchem-1596	51	21	canada	canada	PROPN
eurjchem-1596	51	22	)	)	PUNCT
eurjchem-1596	51	23	.	.	PUNCT
eurjchem-1596	52	1	the	the	DET
eurjchem-1596	52	2	product	product	NOUN
eurjchem-1596	52	3	ion	ion	NOUN
eurjchem-1596	52	4	spectra	spectra	NOUN
eurjchem-1596	52	5	of	of	ADP
eurjchem-1596	52	6	ulipristal	ulipristal	ADJ
eurjchem-1596	52	7	acetate	acetate	NOUN
eurjchem-1596	52	8	and	and	CCONJ
eurjchem-1596	52	9	levonorgestrel	levonorgestrel	NOUN
eurjchem-1596	52	10	are	be	AUX
eurjchem-1596	52	11	shown	show	VERB
eurjchem-1596	52	12	in	in	ADP
eurjchem-1596	52	13	figure	figure	NOUN
eurjchem-1596	52	14	1a	1a	PROPN
eurjchem-1596	52	15	and	and	CCONJ
eurjchem-1596	52	16	b.	b.	PROPN
eurjchem-1596	52	17	calibration	calibration	NOUN
eurjchem-1596	52	18	curves	curve	NOUN
eurjchem-1596	52	19	were	be	AUX
eurjchem-1596	52	20	constructed	construct	VERB
eurjchem-1596	52	21	using	use	VERB
eurjchem-1596	52	22	a	a	DET
eurjchem-1596	52	23	linear	linear	ADJ
eurjchem-1596	52	24	fit	fit	NOUN
eurjchem-1596	52	25	with	with	ADP
eurjchem-1596	52	26	1	1	NUM
eurjchem-1596	52	27	/	/	SYM
eurjchem-1596	52	28	x²	x²	PROPN
eurjchem-1596	52	29	weighting	weighting	NOUN
eurjchem-1596	52	30	,	,	PUNCT
eurjchem-1596	52	31	which	which	PRON
eurjchem-1596	52	32	resulted	result	VERB
eurjchem-1596	52	33	in	in	ADP
eurjchem-1596	52	34	acceptable	acceptable	ADJ
eurjchem-1596	52	35	accuracy	accuracy	NOUN
eurjchem-1596	52	36	over	over	ADP
eurjchem-1596	52	37	the	the	DET
eurjchem-1596	52	38	linear	linear	ADJ
eurjchem-1596	52	39	concentration	concentration	NOUN
eurjchem-1596	52	40	range	range	NOUN
eurjchem-1596	52	41	.	.	PUNCT
eurjchem-1596	53	1	2.3	2.3	NUM
eurjchem-1596	53	2	.	.	PUNCT
eurjchem-1596	53	3	preparation	preparation	NOUN
eurjchem-1596	53	4	of	of	ADP
eurjchem-1596	53	5	stock	stock	NOUN
eurjchem-1596	53	6	solutions	solution	NOUN
eurjchem-1596	53	7	and	and	CCONJ
eurjchem-1596	53	8	working	working	NOUN
eurjchem-1596	53	9	dilutions	dilution	NOUN
eurjchem-1596	53	10	stock	stock	NOUN
eurjchem-1596	53	11	solution	solution	NOUN
eurjchem-1596	53	12	with	with	ADP
eurjchem-1596	53	13	concentration	concentration	NOUN
eurjchem-1596	53	14	of	of	ADP
eurjchem-1596	53	15	approximately	approximately	ADV
eurjchem-1596	53	16	500	500	NUM
eurjchem-1596	53	17	µg	µg	ADV
eurjchem-1596	53	18	/	/	SYM
eurjchem-1596	53	19	ml	ml	NOUN
eurjchem-1596	53	20	was	be	AUX
eurjchem-1596	53	21	prepared	prepare	VERB
eurjchem-1596	53	22	in	in	ADP
eurjchem-1596	53	23	methanol	methanol	NOUN
eurjchem-1596	53	24	for	for	ADP
eurjchem-1596	53	25	both	both	PRON
eurjchem-1596	53	26	analyte	analyte	NOUN
eurjchem-1596	53	27	and	and	CCONJ
eurjchem-1596	53	28	istd	istd	NOUN
eurjchem-1596	53	29	.	.	PUNCT
eurjchem-1596	54	1	serial	serial	ADJ
eurjchem-1596	54	2	spiking	spike	VERB
eurjchem-1596	54	3	dilutions	dilution	NOUN
eurjchem-1596	54	4	of	of	ADP
eurjchem-1596	54	5	analyte	analyte	NOUN
eurjchem-1596	54	6	were	be	AUX
eurjchem-1596	54	7	prepared	prepare	VERB
eurjchem-1596	54	8	in	in	ADP
eurjchem-1596	54	9	the	the	DET
eurjchem-1596	54	10	linear	linear	ADJ
eurjchem-1596	54	11	range	range	NOUN
eurjchem-1596	54	12	of	of	ADP
eurjchem-1596	54	13	1‐300	1‐300	NUM
eurjchem-1596	54	14	ng	ng	PROPN
eurjchem-1596	54	15	/	/	SYM
eurjchem-1596	54	16	ml	ml	VERB
eurjchem-1596	54	17	using	use	VERB
eurjchem-1596	54	18	methanol	methanol	NOUN
eurjchem-1596	54	19	water	water	NOUN
eurjchem-1596	54	20	mixture	mixture	NOUN
eurjchem-1596	54	21	(	(	PUNCT
eurjchem-1596	54	22	80:20	80:20	NUM
eurjchem-1596	54	23	,	,	PUNCT
eurjchem-1596	54	24	v	v	NOUN
eurjchem-1596	54	25	:	:	PUNCT
eurjchem-1596	54	26	v	v	NOUN
eurjchem-1596	54	27	)	)	PUNCT
eurjchem-1596	54	28	as	as	ADP
eurjchem-1596	54	29	diluent	diluent	NOUN
eurjchem-1596	54	30	and	and	CCONJ
eurjchem-1596	54	31	1000	1000	NUM
eurjchem-1596	54	32	ng	ng	PROPN
eurjchem-1596	54	33	/	/	SYM
eurjchem-1596	54	34	ml	ml	X
eurjchem-1596	54	35	of	of	ADP
eurjchem-1596	54	36	levonorgestrel	levonorgestrel	NOUN
eurjchem-1596	54	37	was	be	AUX
eurjchem-1596	54	38	also	also	ADV
eurjchem-1596	54	39	prepared	prepared	ADJ
eurjchem-1596	54	40	to	to	PART
eurjchem-1596	54	41	use	use	VERB
eurjchem-1596	54	42	as	as	ADP
eurjchem-1596	54	43	istd	istd	NOUN
eurjchem-1596	54	44	.	.	PUNCT
eurjchem-1596	55	1	quality	quality	NOUN
eurjchem-1596	55	2	control	control	NOUN
eurjchem-1596	55	3	spiking	spike	VERB
eurjchem-1596	55	4	dilutions	dilution	NOUN
eurjchem-1596	55	5	were	be	AUX
eurjchem-1596	55	6	also	also	ADV
eurjchem-1596	55	7	prepared	prepare	VERB
eurjchem-1596	55	8	using	use	VERB
eurjchem-1596	55	9	different	different	ADJ
eurjchem-1596	55	10	stock	stock	NOUN
eurjchem-1596	55	11	weighing	weighing	NOUN
eurjchem-1596	55	12	.	.	PUNCT
eurjchem-1596	56	1	all	all	DET
eurjchem-1596	56	2	stock	stock	NOUN
eurjchem-1596	56	3	solutions	solution	NOUN
eurjchem-1596	56	4	and	and	CCONJ
eurjchem-1596	56	5	working	working	NOUN
eurjchem-1596	56	6	dilutions	dilution	NOUN
eurjchem-1596	56	7	are	be	AUX
eurjchem-1596	56	8	stored	store	VERB
eurjchem-1596	56	9	in	in	ADP
eurjchem-1596	56	10	refrigeration	refrigeration	NOUN
eurjchem-1596	56	11	at	at	ADP
eurjchem-1596	56	12	2‐8	2‐8	NOUN
eurjchem-1596	56	13	°	°	ADP
eurjchem-1596	56	14	c	c	NOUN
eurjchem-1596	56	15	.	.	PUNCT
eurjchem-1596	57	1	2.4	2.4	NUM
eurjchem-1596	57	2	.	.	PUNCT
eurjchem-1596	57	3	preparation	preparation	NOUN
eurjchem-1596	57	4	of	of	ADP
eurjchem-1596	57	5	calibration	calibration	NOUN
eurjchem-1596	57	6	curve	curve	NOUN
eurjchem-1596	57	7	and	and	CCONJ
eurjchem-1596	57	8	quality	quality	NOUN
eurjchem-1596	57	9	control	control	NOUN
eurjchem-1596	57	10	samples	sample	NOUN
eurjchem-1596	57	11	calibration	calibration	NOUN
eurjchem-1596	57	12	standards	standard	NOUN
eurjchem-1596	57	13	and	and	CCONJ
eurjchem-1596	57	14	qc	qc	PROPN
eurjchem-1596	57	15	samples	sample	NOUN
eurjchem-1596	57	16	were	be	AUX
eurjchem-1596	57	17	prepared	prepare	VERB
eurjchem-1596	57	18	in	in	ADP
eurjchem-1596	57	19	ria	ria	PROPN
eurjchem-1596	57	20	vial	vial	ADJ
eurjchem-1596	57	21	tubes	tube	NOUN
eurjchem-1596	57	22	by	by	ADP
eurjchem-1596	57	23	spiking	spike	VERB
eurjchem-1596	57	24	at	at	ADP
eurjchem-1596	57	25	2	2	NUM
eurjchem-1596	57	26	%	%	NOUN
eurjchem-1596	57	27	(	(	PUNCT
eurjchem-1596	57	28	v	v	NOUN
eurjchem-1596	57	29	:	:	PUNCT
eurjchem-1596	57	30	v	v	NOUN
eurjchem-1596	57	31	)	)	PUNCT
eurjchem-1596	57	32	of	of	ADP
eurjchem-1596	57	33	spiking	spike	VERB
eurjchem-1596	57	34	solution	solution	NOUN
eurjchem-1596	57	35	into	into	ADP
eurjchem-1596	57	36	drug‐free	drug‐free	ADJ
eurjchem-1596	57	37	human	human	ADJ
eurjchem-1596	57	38	plasma	plasma	NOUN
eurjchem-1596	57	39	containing	contain	VERB
eurjchem-1596	57	40	k2edta	k2edta	NOUN
eurjchem-1596	57	41	as	as	ADP
eurjchem-1596	57	42	an	an	DET
eurjchem-1596	57	43	anticoagulant	anticoagulant	NOUN
eurjchem-1596	57	44	.	.	PUNCT
eurjchem-1596	58	1	calibration	calibration	NOUN
eurjchem-1596	58	2	curve	curve	NOUN
eurjchem-1596	58	3	samples	sample	NOUN
eurjchem-1596	58	4	(	(	PUNCT
eurjchem-1596	58	5	cc	cc	NOUN
eurjchem-1596	58	6	1	1	NUM
eurjchem-1596	58	7	to	to	ADP
eurjchem-1596	58	8	cc	cc	PROPN
eurjchem-1596	58	9	8)	8)	NUM
eurjchem-1596	58	10	were	be	AUX
eurjchem-1596	58	11	prepared	prepare	VERB
eurjchem-1596	58	12	across	across	ADP
eurjchem-1596	58	13	the	the	DET
eurjchem-1596	58	14	concentrations	concentration	NOUN
eurjchem-1596	58	15	range	range	VERB
eurjchem-1596	58	16	1‐300	1‐300	NUM
eurjchem-1596	58	17	ng	ng	PROPN
eurjchem-1596	58	18	/	/	SYM
eurjchem-1596	58	19	ml	ml	PROPN
eurjchem-1596	58	20	.	.	PUNCT
eurjchem-1596	58	21	qc	qc	PROPN
eurjchem-1596	58	22	samples	sample	NOUN
eurjchem-1596	58	23	at	at	ADP
eurjchem-1596	58	24	5	5	NUM
eurjchem-1596	58	25	concentration	concentration	NOUN
eurjchem-1596	58	26	levels	level	NOUN
eurjchem-1596	58	27	prepared	prepare	VERB
eurjchem-1596	58	28	as	as	SCONJ
eurjchem-1596	58	29	follows	follow	VERB
eurjchem-1596	58	30	,	,	PUNCT
eurjchem-1596	58	31	lower	low	ADJ
eurjchem-1596	58	32	limit	limit	NOUN
eurjchem-1596	58	33	of	of	ADP
eurjchem-1596	58	34	quantification	quantification	NOUN
eurjchem-1596	58	35	qc	qc	PROPN
eurjchem-1596	58	36	(	(	PUNCT
eurjchem-1596	58	37	lloq	lloq	PROPN
eurjchem-1596	58	38	qc	qc	PROPN
eurjchem-1596	58	39	)	)	PUNCT
eurjchem-1596	58	40	,	,	PUNCT
eurjchem-1596	58	41	1	1	NUM
eurjchem-1596	58	42	ng	ng	PROPN
eurjchem-1596	58	43	/	/	SYM
eurjchem-1596	58	44	ml	ml	PROPN
eurjchem-1596	58	45	;	;	PUNCT
eurjchem-1596	58	46	low	low	PROPN
eurjchem-1596	58	47	qc	qc	PROPN
eurjchem-1596	58	48	(	(	PUNCT
eurjchem-1596	58	49	lqc	lqc	PROPN
eurjchem-1596	58	50	)	)	PUNCT
eurjchem-1596	58	51	,	,	PUNCT
eurjchem-1596	58	52	3	3	NUM
eurjchem-1596	58	53	ng	ng	PROPN
eurjchem-1596	58	54	/	/	SYM
eurjchem-1596	58	55	ml	ml	PROPN
eurjchem-1596	58	56	;	;	PUNCT
eurjchem-1596	58	57	medium	medium	ADJ
eurjchem-1596	58	58	qc	qc	PROPN
eurjchem-1596	58	59	(	(	PUNCT
eurjchem-1596	58	60	mqc	mqc	PROPN
eurjchem-1596	58	61	)	)	PUNCT
eurjchem-1596	58	62	,	,	PUNCT
eurjchem-1596	58	63	126	126	NUM
eurjchem-1596	58	64	ng	ng	NOUN
eurjchem-1596	58	65	/	/	SYM
eurjchem-1596	58	66	ml	ml	PROPN
eurjchem-1596	58	67	;	;	PUNCT
eurjchem-1596	58	68	high	high	ADJ
eurjchem-1596	58	69	qc	qc	PROPN
eurjchem-1596	58	70	(	(	PUNCT
eurjchem-1596	58	71	hqc	hqc	PROPN
eurjchem-1596	58	72	)	)	PUNCT
eurjchem-1596	58	73	,	,	PUNCT
eurjchem-1596	58	74	228	228	NUM
eurjchem-1596	58	75	ng	ng	NOUN
eurjchem-1596	58	76	/	/	SYM
eurjchem-1596	58	77	ml	ml	PROPN
eurjchem-1596	58	78	and	and	CCONJ
eurjchem-1596	58	79	diluted	dilute	VERB
eurjchem-1596	58	80	qc	qc	PROPN
eurjchem-1596	58	81	(	(	PUNCT
eurjchem-1596	58	82	dqc	dqc	PROPN
eurjchem-1596	58	83	)	)	PUNCT
eurjchem-1596	58	84	,	,	PUNCT
eurjchem-1596	58	85	600	600	NUM
eurjchem-1596	58	86	ng	ng	NOUN
eurjchem-1596	58	87	/	/	SYM
eurjchem-1596	58	88	ml	ml	NOUN
eurjchem-1596	58	89	.	.	PUNCT
eurjchem-1596	59	1	all	all	DET
eurjchem-1596	59	2	calibration	calibration	NOUN
eurjchem-1596	59	3	and	and	CCONJ
eurjchem-1596	59	4	qc	qc	PROPN
eurjchem-1596	59	5	plasma	plasma	NOUN
eurjchem-1596	59	6	samples	sample	NOUN
eurjchem-1596	59	7	prepared	prepare	VERB
eurjchem-1596	59	8	in	in	ADP
eurjchem-1596	59	9	ria	ria	PROPN
eurjchem-1596	59	10	vial	vial	ADJ
eurjchem-1596	59	11	tubes	tube	NOUN
eurjchem-1596	59	12	were	be	AUX
eurjchem-1596	59	13	stored	store	VERB
eurjchem-1596	59	14	in	in	ADP
eurjchem-1596	59	15	a	a	DET
eurjchem-1596	59	16	deep	deep	ADJ
eurjchem-1596	59	17	freezer	freezer	NOUN
eurjchem-1596	59	18	at	at	ADP
eurjchem-1596	59	19	‐70	‐70	PROPN
eurjchem-1596	59	20	°	°	ADP
eurjchem-1596	59	21	c	c	NOUN
eurjchem-1596	59	22	until	until	ADP
eurjchem-1596	59	23	analysis	analysis	NOUN
eurjchem-1596	59	24	.	.	PUNCT
eurjchem-1596	60	1	before	before	ADP
eurjchem-1596	60	2	sample	sample	NOUN
eurjchem-1596	60	3	prepa‐	prepa‐	X
eurjchem-1596	60	4	260	260	NUM
eurjchem-1596	60	5	pappula	pappula	NOUN
eurjchem-1596	60	6	et	et	PROPN
eurjchem-1596	60	7	al	al	PROPN
eurjchem-1596	60	8	.	.	PUNCT
eurjchem-1596	60	9	/	/	SYM
eurjchem-1596	60	10	european	european	PROPN
eurjchem-1596	60	11	journal	journal	PROPN
eurjchem-1596	60	12	of	of	ADP
eurjchem-1596	60	13	chemistry	chemistry	NOUN
eurjchem-1596	60	14	8	8	NUM
eurjchem-1596	60	15	(	(	PUNCT
eurjchem-1596	60	16	3	3	NUM
eurjchem-1596	60	17	)	)	PUNCT
eurjchem-1596	60	18	(	(	PUNCT
eurjchem-1596	60	19	2017	2017	NUM
eurjchem-1596	60	20	)	)	PUNCT
eurjchem-1596	60	21	258‐264	258‐264	NUM
eurjchem-1596	60	22	ration	ration	NOUN
eurjchem-1596	60	23	,	,	PUNCT
eurjchem-1596	60	24	samples	sample	NOUN
eurjchem-1596	60	25	were	be	AUX
eurjchem-1596	60	26	retrieved	retrieve	VERB
eurjchem-1596	60	27	from	from	ADP
eurjchem-1596	60	28	the	the	DET
eurjchem-1596	60	29	deep	deep	ADJ
eurjchem-1596	60	30	freezer	freezer	NOUN
eurjchem-1596	60	31	and	and	CCONJ
eurjchem-1596	60	32	thawed	thaw	VERB
eurjchem-1596	60	33	at	at	ADP
eurjchem-1596	60	34	room	room	NOUN
eurjchem-1596	60	35	temperature	temperature	NOUN
eurjchem-1596	60	36	for	for	ADP
eurjchem-1596	60	37	about	about	ADV
eurjchem-1596	60	38	50	50	NUM
eurjchem-1596	60	39	min	min	NOUN
eurjchem-1596	60	40	.	.	PROPN
eurjchem-1596	60	41	2.5	2.5	NUM
eurjchem-1596	60	42	.	.	PUNCT
eurjchem-1596	61	1	sample	sample	NOUN
eurjchem-1596	61	2	extraction	extraction	NOUN
eurjchem-1596	61	3	procedure	procedure	NOUN
eurjchem-1596	61	4	50	50	NUM
eurjchem-1596	61	5	µl	µl	NOUN
eurjchem-1596	61	6	of	of	ADP
eurjchem-1596	61	7	istd	istd	NOUN
eurjchem-1596	61	8	working	work	VERB
eurjchem-1596	61	9	dilution	dilution	NOUN
eurjchem-1596	61	10	(	(	PUNCT
eurjchem-1596	61	11	1000	1000	NUM
eurjchem-1596	61	12	ng	ng	NOUN
eurjchem-1596	61	13	/	/	SYM
eurjchem-1596	61	14	ml	ml	PROPN
eurjchem-1596	61	15	)	)	PUNCT
eurjchem-1596	61	16	was	be	AUX
eurjchem-1596	61	17	added	add	VERB
eurjchem-1596	61	18	to	to	ADP
eurjchem-1596	61	19	a	a	DET
eurjchem-1596	61	20	300	300	NUM
eurjchem-1596	61	21	µl	µl	ADP
eurjchem-1596	61	22	plasma	plasma	NOUN
eurjchem-1596	61	23	sample	sample	NOUN
eurjchem-1596	61	24	in	in	ADP
eurjchem-1596	61	25	a	a	DET
eurjchem-1596	61	26	15	15	NUM
eurjchem-1596	61	27	ml	ml	NOUN
eurjchem-1596	61	28	ria	ria	PROPN
eurjchem-1596	61	29	vial	vial	ADJ
eurjchem-1596	61	30	tube	tube	NOUN
eurjchem-1596	61	31	and	and	CCONJ
eurjchem-1596	61	32	vortexed	vortexe	VERB
eurjchem-1596	61	33	for	for	ADP
eurjchem-1596	61	34	10	10	NUM
eurjchem-1596	61	35	s.	s.	PROPN
eurjchem-1596	61	36	then	then	ADV
eurjchem-1596	61	37	add	add	VERB
eurjchem-1596	61	38	300	300	NUM
eurjchem-1596	61	39	µl	µl	NOUN
eurjchem-1596	61	40	of	of	ADP
eurjchem-1596	61	41	25	25	NUM
eurjchem-1596	61	42	mm	mm	NUM
eurjchem-1596	61	43	sodium	sodium	NOUN
eurjchem-1596	61	44	carbo‐	carbo‐	PROPN
eurjchem-1596	61	45	nate	nate	PROPN
eurjchem-1596	61	46	solution	solution	NOUN
eurjchem-1596	61	47	and	and	CCONJ
eurjchem-1596	61	48	vortexed	vortexe	VERB
eurjchem-1596	61	49	for	for	ADP
eurjchem-1596	61	50	10	10	NUM
eurjchem-1596	61	51	seconds	second	NOUN
eurjchem-1596	61	52	.	.	PUNCT
eurjchem-1596	62	1	add	add	VERB
eurjchem-1596	62	2	3	3	NUM
eurjchem-1596	62	3	ml	ml	NOUN
eurjchem-1596	62	4	extraction	extraction	NOUN
eurjchem-1596	62	5	solvent	solvent	NOUN
eurjchem-1596	62	6	(	(	PUNCT
eurjchem-1596	62	7	n‐hexane	n‐hexane	VERB
eurjchem-1596	62	8	:	:	PUNCT
eurjchem-1596	62	9	methyl	methyl	NOUN
eurjchem-1596	62	10	tert‐butyl	tert‐butyl	ADP
eurjchem-1596	62	11	ether	ether	NOUN
eurjchem-1596	62	12	(	(	PUNCT
eurjchem-1596	62	13	50:50	50:50	NUM
eurjchem-1596	62	14	,	,	PUNCT
eurjchem-1596	62	15	v	v	NOUN
eurjchem-1596	62	16	:	:	PUNCT
eurjchem-1596	62	17	v	v	NOUN
eurjchem-1596	62	18	)	)	PUNCT
eurjchem-1596	62	19	and	and	CCONJ
eurjchem-1596	62	20	vortexed	vortexe	VERB
eurjchem-1596	62	21	for	for	ADP
eurjchem-1596	62	22	10	10	NUM
eurjchem-1596	62	23	min	min	NOUN
eurjchem-1596	62	24	at	at	ADP
eurjchem-1596	62	25	2000	2000	NUM
eurjchem-1596	62	26	rpm	rpm	NOUN
eurjchem-1596	62	27	.	.	PUNCT
eurjchem-1596	63	1	after	after	ADP
eurjchem-1596	63	2	agitation	agitation	NOUN
eurjchem-1596	63	3	,	,	PUNCT
eurjchem-1596	63	4	samples	sample	NOUN
eurjchem-1596	63	5	were	be	AUX
eurjchem-1596	63	6	subjected	subject	VERB
eurjchem-1596	63	7	to	to	PART
eurjchem-1596	63	8	freeze	freeze	VERB
eurjchem-1596	63	9	for	for	ADP
eurjchem-1596	63	10	separating	separate	VERB
eurjchem-1596	63	11	the	the	DET
eurjchem-1596	63	12	extraction	extraction	NOUN
eurjchem-1596	63	13	solvent	solvent	NOUN
eurjchem-1596	63	14	.	.	PUNCT
eurjchem-1596	64	1	the	the	DET
eurjchem-1596	64	2	separated	separate	VERB
eurjchem-1596	64	3	extraction	extraction	NOUN
eurjchem-1596	64	4	solvent	solvent	NOUN
eurjchem-1596	64	5	was	be	AUX
eurjchem-1596	64	6	evaporated	evaporate	VERB
eurjchem-1596	64	7	for	for	ADP
eurjchem-1596	64	8	20	20	NUM
eurjchem-1596	64	9	min	min	NOUN
eurjchem-1596	64	10	under	under	ADP
eurjchem-1596	64	11	dry	dry	ADJ
eurjchem-1596	64	12	nitrogen	nitrogen	NOUN
eurjchem-1596	64	13	gas	gas	NOUN
eurjchem-1596	64	14	at	at	ADP
eurjchem-1596	64	15	pressure	pressure	NOUN
eurjchem-1596	64	16	of	of	ADP
eurjchem-1596	64	17	20	20	NUM
eurjchem-1596	64	18	psi	psi	NOUN
eurjchem-1596	64	19	.	.	PUNCT
eurjchem-1596	65	1	after	after	ADP
eurjchem-1596	65	2	evaporation	evaporation	NOUN
eurjchem-1596	65	3	the	the	DET
eurjchem-1596	65	4	samples	sample	NOUN
eurjchem-1596	65	5	were	be	AUX
eurjchem-1596	65	6	reconstituted	reconstitute	VERB
eurjchem-1596	65	7	with	with	ADP
eurjchem-1596	65	8	200	200	NUM
eurjchem-1596	65	9	µl	µl	NOUN
eurjchem-1596	65	10	of	of	ADP
eurjchem-1596	65	11	mobile	mobile	ADJ
eurjchem-1596	65	12	phase	phase	NOUN
eurjchem-1596	65	13	and	and	CCONJ
eurjchem-1596	65	14	15	15	NUM
eurjchem-1596	65	15	µl	µl	NOUN
eurjchem-1596	65	16	was	be	AUX
eurjchem-1596	65	17	injected	inject	VERB
eurjchem-1596	65	18	into	into	ADP
eurjchem-1596	65	19	lc‐ms	lc‐ms	AUX
eurjchem-1596	65	20	/	/	SYM
eurjchem-1596	65	21	ms	ms	NOUN
eurjchem-1596	65	22	system	system	NOUN
eurjchem-1596	65	23	for	for	ADP
eurjchem-1596	65	24	analysis	analysis	NOUN
eurjchem-1596	65	25	.	.	PUNCT
eurjchem-1596	66	1	3	3	X
eurjchem-1596	66	2	.	.	NOUN
eurjchem-1596	66	3	results	result	NOUN
eurjchem-1596	66	4	and	and	CCONJ
eurjchem-1596	66	5	discussion	discussion	NOUN
eurjchem-1596	66	6	3.1	3.1	NUM
eurjchem-1596	66	7	.	.	PUNCT
eurjchem-1596	67	1	method	method	NOUN
eurjchem-1596	67	2	development	development	NOUN
eurjchem-1596	67	3	3.1.1	3.1.1	NOUN
eurjchem-1596	67	4	.	.	PUNCT
eurjchem-1596	68	1	selection	selection	NOUN
eurjchem-1596	68	2	of	of	ADP
eurjchem-1596	68	3	internal	internal	ADJ
eurjchem-1596	68	4	standard	standard	NOUN
eurjchem-1596	68	5	it	it	PRON
eurjchem-1596	68	6	is	be	AUX
eurjchem-1596	68	7	very	very	ADV
eurjchem-1596	68	8	important	important	ADJ
eurjchem-1596	68	9	to	to	PART
eurjchem-1596	68	10	choose	choose	VERB
eurjchem-1596	68	11	an	an	DET
eurjchem-1596	68	12	appropriate	appropriate	ADJ
eurjchem-1596	68	13	istd	istd	NOUN
eurjchem-1596	68	14	to	to	PART
eurjchem-1596	68	15	achieve	achieve	VERB
eurjchem-1596	68	16	high	high	ADJ
eurjchem-1596	68	17	accuracy	accuracy	NOUN
eurjchem-1596	68	18	and	and	CCONJ
eurjchem-1596	68	19	precision	precision	NOUN
eurjchem-1596	68	20	in	in	ADP
eurjchem-1596	68	21	the	the	DET
eurjchem-1596	68	22	quantification	quantification	NOUN
eurjchem-1596	68	23	assay	assay	VERB
eurjchem-1596	68	24	by	by	ADP
eurjchem-1596	68	25	lc‐ms	lc‐ms	AUX
eurjchem-1596	68	26	/	/	SYM
eurjchem-1596	68	27	ms	ms	PROPN
eurjchem-1596	68	28	.	.	PROPN
eurjchem-1596	68	29	as	as	SCONJ
eurjchem-1596	68	30	generally	generally	ADV
eurjchem-1596	68	31	speaking	speak	VERB
eurjchem-1596	68	32	,	,	PUNCT
eurjchem-1596	68	33	isotope	isotope	NOUN
eurjchem-1596	68	34	labelled	label	VERB
eurjchem-1596	68	35	internal	internal	ADJ
eurjchem-1596	68	36	standards	standard	NOUN
eurjchem-1596	68	37	are	be	AUX
eurjchem-1596	68	38	expensive	expensive	ADJ
eurjchem-1596	68	39	and	and	CCONJ
eurjchem-1596	68	40	escalate	escalate	VERB
eurjchem-1596	68	41	the	the	DET
eurjchem-1596	68	42	cost	cost	NOUN
eurjchem-1596	68	43	of	of	ADP
eurjchem-1596	68	44	analysis	analysis	NOUN
eurjchem-1596	68	45	that	that	PRON
eurjchem-1596	68	46	limits	limit	VERB
eurjchem-1596	68	47	the	the	DET
eurjchem-1596	68	48	usage	usage	NOUN
eurjchem-1596	68	49	of	of	ADP
eurjchem-1596	68	50	isotope	isotope	NOUN
eurjchem-1596	68	51	labelled	label	VERB
eurjchem-1596	68	52	istd	istd	NOUN
eurjchem-1596	68	53	.	.	PUNCT
eurjchem-1596	69	1	hence	hence	ADV
eurjchem-1596	69	2	for	for	ADP
eurjchem-1596	69	3	developing	develop	VERB
eurjchem-1596	69	4	cost	cost	NOUN
eurjchem-1596	69	5	effective	effective	ADJ
eurjchem-1596	69	6	method	method	NOUN
eurjchem-1596	69	7	,	,	PUNCT
eurjchem-1596	69	8	levonorgestrel	levonorgestrel	NOUN
eurjchem-1596	69	9	is	be	AUX
eurjchem-1596	69	10	selected	select	VERB
eurjchem-1596	69	11	as	as	ADP
eurjchem-1596	69	12	internal	internal	ADJ
eurjchem-1596	69	13	standard	standard	NOUN
eurjchem-1596	69	14	,	,	PUNCT
eurjchem-1596	69	15	which	which	PRON
eurjchem-1596	69	16	was	be	AUX
eurjchem-1596	69	17	found	find	VERB
eurjchem-1596	69	18	to	to	PART
eurjchem-1596	69	19	have	have	VERB
eurjchem-1596	69	20	almost	almost	ADV
eurjchem-1596	69	21	similar	similar	ADJ
eurjchem-1596	69	22	behaviour	behaviour	NOUN
eurjchem-1596	69	23	(	(	PUNCT
eurjchem-1596	69	24	chemical	chemical	NOUN
eurjchem-1596	69	25	structure	structure	NOUN
eurjchem-1596	69	26	and	and	CCONJ
eurjchem-1596	69	27	ionisation	ionisation	NOUN
eurjchem-1596	69	28	)	)	PUNCT
eurjchem-1596	69	29	and	and	CCONJ
eurjchem-1596	69	30	co‐eluting	co‐elute	VERB
eurjchem-1596	69	31	properties	property	NOUN
eurjchem-1596	69	32	as	as	ADP
eurjchem-1596	69	33	analyte	analyte	NOUN
eurjchem-1596	69	34	.	.	PUNCT
eurjchem-1596	70	1	levonorgestrel	levonorgestrel	NOUN
eurjchem-1596	70	2	also	also	ADV
eurjchem-1596	70	3	has	have	VERB
eurjchem-1596	70	4	similar	similar	ADJ
eurjchem-1596	70	5	extraction	extraction	NOUN
eurjchem-1596	70	6	efficiency	efficiency	NOUN
eurjchem-1596	70	7	in	in	ADP
eurjchem-1596	70	8	optimized	optimize	VERB
eurjchem-1596	70	9	conditions	condition	NOUN
eurjchem-1596	70	10	and	and	CCONJ
eurjchem-1596	70	11	because	because	SCONJ
eurjchem-1596	70	12	of	of	ADP
eurjchem-1596	70	13	its	its	PRON
eurjchem-1596	70	14	negligible	negligible	ADJ
eurjchem-1596	70	15	matrix	matrix	NOUN
eurjchem-1596	70	16	effect	effect	NOUN
eurjchem-1596	70	17	renders	render	VERB
eurjchem-1596	70	18	it	it	PRON
eurjchem-1596	70	19	suitable	suitable	ADJ
eurjchem-1596	70	20	as	as	ADP
eurjchem-1596	70	21	internal	internal	ADJ
eurjchem-1596	70	22	standard	standard	NOUN
eurjchem-1596	70	23	.	.	PUNCT
eurjchem-1596	71	1	there‐	there‐	NOUN
eurjchem-1596	71	2	fore	fore	NOUN
eurjchem-1596	71	3	,	,	PUNCT
eurjchem-1596	71	4	it	it	PRON
eurjchem-1596	71	5	was	be	AUX
eurjchem-1596	71	6	selected	select	VERB
eurjchem-1596	71	7	as	as	ADP
eurjchem-1596	71	8	internal	internal	ADJ
eurjchem-1596	71	9	standard	standard	NOUN
eurjchem-1596	71	10	for	for	ADP
eurjchem-1596	71	11	all	all	DET
eurjchem-1596	71	12	experiments	experiment	NOUN
eurjchem-1596	71	13	.	.	PUNCT
eurjchem-1596	72	1	3.1.2	3.1.2	NUM
eurjchem-1596	72	2	.	.	PUNCT
eurjchem-1596	72	3	lc‐ms	lc‐ms	AUX
eurjchem-1596	72	4	/	/	SYM
eurjchem-1596	73	1	ms	ms	PROPN
eurjchem-1596	73	2	conditions	condition	NOUN
eurjchem-1596	73	3	ms	ms	PROPN
eurjchem-1596	73	4	/	/	SYM
eurjchem-1596	73	5	ms	ms	PROPN
eurjchem-1596	73	6	parameters	parameter	NOUN
eurjchem-1596	73	7	were	be	AUX
eurjchem-1596	73	8	optimized	optimize	VERB
eurjchem-1596	73	9	by	by	ADP
eurjchem-1596	73	10	continuous	continuous	ADJ
eurjchem-1596	73	11	infusing	infusing	NOUN
eurjchem-1596	73	12	of	of	ADP
eurjchem-1596	73	13	analyte	analyte	NOUN
eurjchem-1596	73	14	and	and	CCONJ
eurjchem-1596	73	15	istd	istd	NOUN
eurjchem-1596	73	16	(	(	PUNCT
eurjchem-1596	73	17	500	500	NUM
eurjchem-1596	73	18	ng	ng	NOUN
eurjchem-1596	73	19	/	/	SYM
eurjchem-1596	73	20	ml	ml	NOUN
eurjchem-1596	73	21	)	)	PUNCT
eurjchem-1596	73	22	into	into	ADP
eurjchem-1596	73	23	electrospray	electrospray	ADJ
eurjchem-1596	73	24	ionisation	ionisation	NOUN
eurjchem-1596	73	25	(	(	PUNCT
eurjchem-1596	73	26	esi	esi	NOUN
eurjchem-1596	73	27	)	)	PUNCT
eurjchem-1596	73	28	source	source	NOUN
eurjchem-1596	73	29	.	.	PUNCT
eurjchem-1596	74	1	it	it	PRON
eurjchem-1596	74	2	was	be	AUX
eurjchem-1596	74	3	found	find	VERB
eurjchem-1596	74	4	that	that	SCONJ
eurjchem-1596	74	5	positive‐ion	positive‐ion	NOUN
eurjchem-1596	74	6	mode	mode	NOUN
eurjchem-1596	74	7	exhibits	exhibit	VERB
eurjchem-1596	74	8	greater	great	ADJ
eurjchem-1596	74	9	sensitivity	sensitivity	NOUN
eurjchem-1596	74	10	for	for	ADP
eurjchem-1596	74	11	analyte	analyte	NOUN
eurjchem-1596	74	12	and	and	CCONJ
eurjchem-1596	74	13	internal	internal	ADJ
eurjchem-1596	74	14	standard	standard	NOUN
eurjchem-1596	74	15	.	.	PUNCT
eurjchem-1596	75	1	tuning	tuning	NOUN
eurjchem-1596	75	2	and	and	CCONJ
eurjchem-1596	75	3	optimization	optimization	NOUN
eurjchem-1596	75	4	of	of	ADP
eurjchem-1596	75	5	compound	compound	NOUN
eurjchem-1596	75	6	parameters	parameter	NOUN
eurjchem-1596	75	7	(	(	PUNCT
eurjchem-1596	75	8	declustering	declustere	VERB
eurjchem-1596	75	9	potential	potential	NOUN
eurjchem-1596	75	10	;	;	PUNCT
eurjchem-1596	75	11	dp	dp	NOUN
eurjchem-1596	75	12	,	,	PUNCT
eurjchem-1596	75	13	entrance	entrance	NOUN
eurjchem-1596	75	14	potential	potential	NOUN
eurjchem-1596	75	15	;	;	PUNCT
eurjchem-1596	75	16	ep	ep	NOUN
eurjchem-1596	75	17	,	,	PUNCT
eurjchem-1596	75	18	collision	collision	NOUN
eurjchem-1596	75	19	energy	energy	NOUN
eurjchem-1596	75	20	;	;	PUNCT
eurjchem-1596	75	21	ce	ce	PROPN
eurjchem-1596	75	22	,	,	PUNCT
eurjchem-1596	75	23	collision	collision	NOUN
eurjchem-1596	75	24	cell	cell	NOUN
eurjchem-1596	75	25	exit	exit	NOUN
eurjchem-1596	75	26	potential	potential	NOUN
eurjchem-1596	75	27	;	;	PUNCT
eurjchem-1596	75	28	cxp	cxp	PROPN
eurjchem-1596	75	29	)	)	PUNCT
eurjchem-1596	75	30	was	be	AUX
eurjchem-1596	75	31	done	do	VERB
eurjchem-1596	75	32	for	for	ADP
eurjchem-1596	75	33	selecting	select	VERB
eurjchem-1596	75	34	ion	ion	NOUN
eurjchem-1596	75	35	transitions	transition	NOUN
eurjchem-1596	75	36	for	for	ADP
eurjchem-1596	75	37	both	both	CCONJ
eurjchem-1596	75	38	parent	parent	NOUN
eurjchem-1596	75	39	and	and	CCONJ
eurjchem-1596	75	40	product	product	NOUN
eurjchem-1596	75	41	ions	ion	NOUN
eurjchem-1596	75	42	for	for	ADP
eurjchem-1596	75	43	mrm	mrm	PROPN
eurjchem-1596	75	44	.	.	PUNCT
eurjchem-1596	76	1	finally	finally	ADV
eurjchem-1596	76	2	source	source	VERB
eurjchem-1596	76	3	parameters	parameter	NOUN
eurjchem-1596	76	4	for	for	ADP
eurjchem-1596	76	5	multiple	multiple	ADJ
eurjchem-1596	76	6	reactions	reaction	NOUN
eurjchem-1596	76	7	monitoring	monitor	VERB
eurjchem-1596	76	8	(	(	PUNCT
eurjchem-1596	76	9	mrm	mrm	PROPN
eurjchem-1596	76	10	)	)	PUNCT
eurjchem-1596	76	11	were	be	AUX
eurjchem-1596	76	12	optimized	optimize	VERB
eurjchem-1596	76	13	by	by	ADP
eurjchem-1596	76	14	infusing	infuse	VERB
eurjchem-1596	76	15	analyte	analyte	NOUN
eurjchem-1596	76	16	and	and	CCONJ
eurjchem-1596	76	17	istd	istd	NOUN
eurjchem-1596	76	18	along	along	ADP
eurjchem-1596	76	19	with	with	ADP
eurjchem-1596	76	20	mobile	mobile	ADJ
eurjchem-1596	76	21	phase	phase	NOUN
eurjchem-1596	76	22	.	.	PUNCT
eurjchem-1596	77	1	the	the	DET
eurjchem-1596	77	2	chromatographic	chromatographic	ADJ
eurjchem-1596	77	3	conditions	condition	NOUN
eurjchem-1596	77	4	were	be	AUX
eurjchem-1596	77	5	optimized	optimize	VERB
eurjchem-1596	77	6	primarily	primarily	ADV
eurjchem-1596	77	7	on	on	ADP
eurjchem-1596	77	8	composition	composition	NOUN
eurjchem-1596	77	9	of	of	ADP
eurjchem-1596	77	10	mobile	mobile	ADJ
eurjchem-1596	77	11	phase	phase	NOUN
eurjchem-1596	77	12	.	.	PUNCT
eurjchem-1596	78	1	analyte	analyte	NOUN
eurjchem-1596	78	2	and	and	CCONJ
eurjchem-1596	78	3	istd	istd	NOUN
eurjchem-1596	78	4	were	be	AUX
eurjchem-1596	78	5	injected	inject	VERB
eurjchem-1596	78	6	initially	initially	ADV
eurjchem-1596	78	7	using	use	VERB
eurjchem-1596	78	8	mobile	mobile	ADJ
eurjchem-1596	78	9	phase	phase	NOUN
eurjchem-1596	78	10	consisting	consist	VERB
eurjchem-1596	78	11	mixture	mixture	NOUN
eurjchem-1596	78	12	of	of	ADP
eurjchem-1596	78	13	acetonitrile	acetonitrile	NOUN
eurjchem-1596	78	14	,	,	PUNCT
eurjchem-1596	78	15	10	10	NUM
eurjchem-1596	78	16	mm	mm	NOUN
eurjchem-1596	78	17	ammonium	ammonium	NOUN
eurjchem-1596	78	18	formate	formate	NOUN
eurjchem-1596	78	19	70:30	70:30	NUM
eurjchem-1596	78	20	(	(	PUNCT
eurjchem-1596	78	21	v	v	NOUN
eurjchem-1596	78	22	:	:	PUNCT
eurjchem-1596	78	23	v	v	NOUN
eurjchem-1596	78	24	)	)	PUNCT
eurjchem-1596	78	25	on	on	ADP
eurjchem-1596	78	26	zorbax	zorbax	PROPN
eurjchem-1596	78	27	c18	c18	PROPN
eurjchem-1596	78	28	(	(	PUNCT
eurjchem-1596	78	29	5	5	NUM
eurjchem-1596	78	30	µm	µm	NOUN
eurjchem-1596	78	31	,	,	PUNCT
eurjchem-1596	78	32	50×4.6	50×4.6	PROPN
eurjchem-1596	78	33	mm	mm	NOUN
eurjchem-1596	78	34	,	,	PUNCT
eurjchem-1596	78	35	i.d	i.d	PROPN
eurjchem-1596	78	36	.	.	PROPN
eurjchem-1596	78	37	)	)	PUNCT
eurjchem-1596	78	38	.	.	PUNCT
eurjchem-1596	79	1	the	the	DET
eurjchem-1596	79	2	chromatographic	chromatographic	ADJ
eurjchem-1596	79	3	retention	retention	NOUN
eurjchem-1596	79	4	was	be	AUX
eurjchem-1596	79	5	at	at	ADP
eurjchem-1596	79	6	4	4	NUM
eurjchem-1596	79	7	min	min	NOUN
eurjchem-1596	79	8	and	and	CCONJ
eurjchem-1596	79	9	the	the	DET
eurjchem-1596	79	10	peak	peak	NOUN
eurjchem-1596	79	11	is	be	AUX
eurjchem-1596	79	12	broad	broad	ADJ
eurjchem-1596	79	13	.	.	PUNCT
eurjchem-1596	80	1	to	to	PART
eurjchem-1596	80	2	achieve	achieve	VERB
eurjchem-1596	80	3	good	good	ADJ
eurjchem-1596	80	4	peak	peak	NOUN
eurjchem-1596	80	5	shape	shape	NOUN
eurjchem-1596	80	6	,	,	PUNCT
eurjchem-1596	80	7	the	the	DET
eurjchem-1596	80	8	required	require	VERB
eurjchem-1596	80	9	sensitivity	sensitivity	NOUN
eurjchem-1596	80	10	at	at	ADP
eurjchem-1596	80	11	lloq	lloq	NOUN
eurjchem-1596	80	12	level	level	NOUN
eurjchem-1596	80	13	and	and	CCONJ
eurjchem-1596	80	14	to	to	PART
eurjchem-1596	80	15	reduce	reduce	VERB
eurjchem-1596	80	16	the	the	DET
eurjchem-1596	80	17	run	run	NOUN
eurjchem-1596	80	18	time	time	NOUN
eurjchem-1596	80	19	the	the	DET
eurjchem-1596	80	20	aqueous	aqueous	ADJ
eurjchem-1596	80	21	buffer	buffer	NOUN
eurjchem-1596	80	22	was	be	AUX
eurjchem-1596	80	23	adjusted	adjust	VERB
eurjchem-1596	80	24	with	with	ADP
eurjchem-1596	80	25	formic	formic	ADJ
eurjchem-1596	80	26	acid	acid	NOUN
eurjchem-1596	80	27	to	to	ADP
eurjchem-1596	80	28	ph	ph	ADJ
eurjchem-1596	80	29	=	=	NOUN
eurjchem-1596	80	30	3.5	3.5	NUM
eurjchem-1596	80	31	from	from	ADP
eurjchem-1596	80	32	initial	initial	ADJ
eurjchem-1596	80	33	value	value	NOUN
eurjchem-1596	80	34	.	.	PUNCT
eurjchem-1596	81	1	compared	compare	VERB
eurjchem-1596	81	2	to	to	ADP
eurjchem-1596	81	3	methanol	methanol	NOUN
eurjchem-1596	81	4	,	,	PUNCT
eurjchem-1596	81	5	acetonitrile	acetonitrile	NOUN
eurjchem-1596	81	6	90	90	NUM
eurjchem-1596	81	7	%	%	NOUN
eurjchem-1596	81	8	as	as	ADP
eurjchem-1596	81	9	organic	organic	ADJ
eurjchem-1596	81	10	modifier	modifier	NOUN
eurjchem-1596	81	11	gives	give	VERB
eurjchem-1596	81	12	highest	high	ADJ
eurjchem-1596	81	13	sensitivity	sensitivity	NOUN
eurjchem-1596	81	14	.	.	PUNCT
eurjchem-1596	82	1	several	several	ADJ
eurjchem-1596	82	2	columns	column	NOUN
eurjchem-1596	82	3	were	be	AUX
eurjchem-1596	82	4	screened	screen	VERB
eurjchem-1596	82	5	,	,	PUNCT
eurjchem-1596	82	6	finally	finally	ADV
eurjchem-1596	82	7	kinetex	kinetex	VERB
eurjchem-1596	82	8	evo	evo	PROPN
eurjchem-1596	82	9	c18	c18	PROPN
eurjchem-1596	82	10	(	(	PUNCT
eurjchem-1596	82	11	5	5	NUM
eurjchem-1596	82	12	µm	µm	NOUN
eurjchem-1596	82	13	,	,	PUNCT
eurjchem-1596	82	14	50×4.6	50×4.6	PROPN
eurjchem-1596	82	15	mm	mm	NOUN
eurjchem-1596	82	16	,	,	PUNCT
eurjchem-1596	82	17	i.d	i.d	PROPN
eurjchem-1596	82	18	.	.	PROPN
eurjchem-1596	82	19	)	)	PUNCT
eurjchem-1596	82	20	was	be	AUX
eurjchem-1596	82	21	selected	select	VERB
eurjchem-1596	82	22	as	as	ADP
eurjchem-1596	82	23	a	a	DET
eurjchem-1596	82	24	result	result	NOUN
eurjchem-1596	82	25	of	of	ADP
eurjchem-1596	82	26	its	its	PRON
eurjchem-1596	82	27	less	less	ADJ
eurjchem-1596	82	28	retention	retention	NOUN
eurjchem-1596	82	29	time	time	NOUN
eurjchem-1596	82	30	with	with	ADP
eurjchem-1596	82	31	acceptable	acceptable	ADJ
eurjchem-1596	82	32	peak	peak	NOUN
eurjchem-1596	82	33	shape	shape	NOUN
eurjchem-1596	82	34	.	.	PUNCT
eurjchem-1596	83	1	3.1.3	3.1.3	X
eurjchem-1596	83	2	.	.	PUNCT
eurjchem-1596	83	3	optimizing	optimize	VERB
eurjchem-1596	83	4	sample	sample	NOUN
eurjchem-1596	83	5	preparation	preparation	NOUN
eurjchem-1596	83	6	protein	protein	NOUN
eurjchem-1596	83	7	precipitation	precipitation	NOUN
eurjchem-1596	83	8	,	,	PUNCT
eurjchem-1596	83	9	lle	lle	PROPN
eurjchem-1596	83	10	has	have	AUX
eurjchem-1596	83	11	been	be	AUX
eurjchem-1596	83	12	checked	check	VERB
eurjchem-1596	83	13	for	for	ADP
eurjchem-1596	83	14	sample	sample	NOUN
eurjchem-1596	83	15	preparation	preparation	NOUN
eurjchem-1596	83	16	.	.	PUNCT
eurjchem-1596	84	1	protein	protein	NOUN
eurjchem-1596	84	2	precipitation	precipitation	NOUN
eurjchem-1596	84	3	is	be	AUX
eurjchem-1596	84	4	simple	simple	ADJ
eurjchem-1596	84	5	but	but	CCONJ
eurjchem-1596	84	6	levonorgestrel	levonorgestrel	NOUN
eurjchem-1596	84	7	shows	show	VERB
eurjchem-1596	84	8	matrix	matrix	NOUN
eurjchem-1596	84	9	effect	effect	NOUN
eurjchem-1596	84	10	over	over	ADP
eurjchem-1596	84	11	80	80	NUM
eurjchem-1596	84	12	%	%	NOUN
eurjchem-1596	84	13	.	.	PUNCT
eurjchem-1596	85	1	in	in	ADP
eurjchem-1596	85	2	consequence	consequence	NOUN
eurjchem-1596	85	3	,	,	PUNCT
eurjchem-1596	85	4	lle	lle	PROPN
eurjchem-1596	85	5	was	be	AUX
eurjchem-1596	85	6	chosen	choose	VERB
eurjchem-1596	85	7	to	to	PART
eurjchem-1596	85	8	prepare	prepare	VERB
eurjchem-1596	85	9	samples	sample	NOUN
eurjchem-1596	85	10	for	for	ADP
eurjchem-1596	85	11	benefit	benefit	NOUN
eurjchem-1596	85	12	of	of	ADP
eurjchem-1596	85	13	specificity	specificity	NOUN
eurjchem-1596	85	14	and	and	CCONJ
eurjchem-1596	85	15	cleanliness	cleanliness	NOUN
eurjchem-1596	85	16	.	.	PUNCT
eurjchem-1596	86	1	methyl	methyl	NOUN
eurjchem-1596	86	2	tertiary	tertiary	ADJ
eurjchem-1596	86	3	butyl	butyl	NOUN
eurjchem-1596	86	4	ether	ether	NOUN
eurjchem-1596	86	5	,	,	PUNCT
eurjchem-1596	86	6	diethyl	diethyl	NOUN
eurjchem-1596	86	7	ether	ether	NOUN
eurjchem-1596	86	8	,	,	PUNCT
eurjchem-1596	86	9	ethyl	ethyl	PROPN
eurjchem-1596	86	10	acetate‐hexane	acetate‐hexane	PROPN
eurjchem-1596	86	11	were	be	AUX
eurjchem-1596	86	12	attempted	attempt	VERB
eurjchem-1596	86	13	individually	individually	ADV
eurjchem-1596	86	14	and	and	CCONJ
eurjchem-1596	86	15	also	also	ADV
eurjchem-1596	86	16	as	as	ADP
eurjchem-1596	86	17	solvent	solvent	ADJ
eurjchem-1596	86	18	mixtures	mixture	NOUN
eurjchem-1596	86	19	.	.	PUNCT
eurjchem-1596	87	1	finally	finally	ADV
eurjchem-1596	87	2	n‐hexane	n‐hexane	ADP
eurjchem-1596	87	3	:	:	PUNCT
eurjchem-1596	87	4	methyl	methyl	NOUN
eurjchem-1596	87	5	tert‐butyl	tert‐butyl	ADP
eurjchem-1596	87	6	ether	ether	NOUN
eurjchem-1596	87	7	in	in	ADP
eurjchem-1596	87	8	the	the	DET
eurjchem-1596	87	9	ratio	ratio	NOUN
eurjchem-1596	87	10	of	of	ADP
eurjchem-1596	87	11	50:50	50:50	NUM
eurjchem-1596	87	12	(	(	PUNCT
eurjchem-1596	87	13	v	v	NOUN
eurjchem-1596	87	14	:	:	PUNCT
eurjchem-1596	87	15	v	v	NOUN
eurjchem-1596	87	16	)	)	PUNCT
eurjchem-1596	87	17	was	be	AUX
eurjchem-1596	87	18	selected	select	VERB
eurjchem-1596	87	19	as	as	ADP
eurjchem-1596	87	20	extraction	extraction	NOUN
eurjchem-1596	87	21	solvent	solvent	NOUN
eurjchem-1596	87	22	because	because	SCONJ
eurjchem-1596	87	23	of	of	ADP
eurjchem-1596	87	24	its	its	PRON
eurjchem-1596	87	25	high	high	ADJ
eurjchem-1596	87	26	and	and	CCONJ
eurjchem-1596	87	27	similar	similar	ADJ
eurjchem-1596	87	28	extraction	extraction	NOUN
eurjchem-1596	87	29	recovery	recovery	NOUN
eurjchem-1596	87	30	for	for	ADP
eurjchem-1596	87	31	analyte	analyte	NOUN
eurjchem-1596	87	32	and	and	CCONJ
eurjchem-1596	87	33	istd	istd	NOUN
eurjchem-1596	87	34	with	with	ADP
eurjchem-1596	87	35	negligible	negligible	ADJ
eurjchem-1596	87	36	matrix	matrix	NOUN
eurjchem-1596	87	37	effect	effect	NOUN
eurjchem-1596	87	38	.	.	PUNCT
eurjchem-1596	88	1	3.2	3.2	NUM
eurjchem-1596	88	2	.	.	PUNCT
eurjchem-1596	89	1	method	method	NOUN
eurjchem-1596	89	2	validation	validation	NOUN
eurjchem-1596	89	3	method	method	NOUN
eurjchem-1596	89	4	validation	validation	NOUN
eurjchem-1596	89	5	for	for	ADP
eurjchem-1596	89	6	analysis	analysis	NOUN
eurjchem-1596	89	7	of	of	ADP
eurjchem-1596	89	8	ulipristal	ulipristal	ADJ
eurjchem-1596	89	9	acetate	acetate	NOUN
eurjchem-1596	89	10	in	in	ADP
eurjchem-1596	89	11	human	human	ADJ
eurjchem-1596	89	12	plasma	plasma	NOUN
eurjchem-1596	89	13	has	have	AUX
eurjchem-1596	89	14	been	be	AUX
eurjchem-1596	89	15	carried	carry	VERB
eurjchem-1596	89	16	out	out	ADP
eurjchem-1596	89	17	in	in	ADP
eurjchem-1596	89	18	compliance	compliance	NOUN
eurjchem-1596	89	19	with	with	ADP
eurjchem-1596	89	20	the	the	DET
eurjchem-1596	89	21	us‐	us‐	PROPN
eurjchem-1596	89	22	fda	fda	PROPN
eurjchem-1596	89	23	and	and	CCONJ
eurjchem-1596	89	24	anvisa	anvisa	PROPN
eurjchem-1596	89	25	resolution	resolution	PROPN
eurjchem-1596	89	26	(	(	PUNCT
eurjchem-1596	89	27	brazil	brazil	PROPN
eurjchem-1596	89	28	)	)	PUNCT
eurjchem-1596	89	29	guidelines	guideline	NOUN
eurjchem-1596	89	30	[	[	X
eurjchem-1596	89	31	9,10	9,10	X
eurjchem-1596	89	32	]	]	X
eurjchem-1596	89	33	as	as	ADP
eurjchem-1596	89	34	per	per	ADP
eurjchem-1596	89	35	method	method	NOUN
eurjchem-1596	89	36	validation	validation	NOUN
eurjchem-1596	89	37	plan	plan	NOUN
eurjchem-1596	89	38	.	.	PUNCT
eurjchem-1596	90	1	results	result	NOUN
eurjchem-1596	90	2	were	be	AUX
eurjchem-1596	90	3	evaluated	evaluate	VERB
eurjchem-1596	90	4	for	for	ADP
eurjchem-1596	90	5	precision	precision	NOUN
eurjchem-1596	90	6	(	(	PUNCT
eurjchem-1596	90	7	cv	cv	PROPN
eurjchem-1596	90	8	≤	≤	NUM
eurjchem-1596	90	9	15	15	NUM
eurjchem-1596	90	10	%	%	NOUN
eurjchem-1596	90	11	;	;	PUNCT
eurjchem-1596	90	12	lloq	lloq	NOUN
eurjchem-1596	90	13	and	and	CCONJ
eurjchem-1596	90	14	lloq	lloq	PROPN
eurjchem-1596	90	15	qc	qc	PROPN
eurjchem-1596	90	16	:	:	PUNCT
eurjchem-1596	90	17	cv	cv	PROPN
eurjchem-1596	90	18	≤	≤	NUM
eurjchem-1596	90	19	20	20	NUM
eurjchem-1596	90	20	%	%	NOUN
eurjchem-1596	90	21	)	)	PUNCT
eurjchem-1596	90	22	and	and	CCONJ
eurjchem-1596	90	23	accuracy	accuracy	NOUN
eurjchem-1596	90	24	(	(	PUNCT
eurjchem-1596	90	25	back	back	ADV
eurjchem-1596	90	26	calculated	calculated	ADJ
eurjchem-1596	90	27	concentrations	concentration	NOUN
eurjchem-1596	90	28	within	within	ADP
eurjchem-1596	90	29	85‐115	85‐115	NUM
eurjchem-1596	90	30	%	%	NOUN
eurjchem-1596	90	31	;	;	PUNCT
eurjchem-1596	90	32	lloq	lloq	NOUN
eurjchem-1596	90	33	and	and	CCONJ
eurjchem-1596	90	34	lloqqc	lloqqc	NOUN
eurjchem-1596	90	35	:	:	PUNCT
eurjchem-1596	90	36	80‐120	80‐120	NUM
eurjchem-1596	90	37	%	%	NOUN
eurjchem-1596	90	38	compared	compare	VERB
eurjchem-1596	90	39	to	to	ADP
eurjchem-1596	90	40	nominal	nominal	ADJ
eurjchem-1596	90	41	concentrations	concentration	NOUN
eurjchem-1596	90	42	)	)	PUNCT
eurjchem-1596	90	43	.	.	PUNCT
eurjchem-1596	91	1	all	all	DET
eurjchem-1596	91	2	plasma	plasma	NOUN
eurjchem-1596	91	3	stability	stability	NOUN
eurjchem-1596	91	4	experiments	experiment	NOUN
eurjchem-1596	91	5	were	be	AUX
eurjchem-1596	91	6	carried	carry	VERB
eurjchem-1596	91	7	out	out	ADP
eurjchem-1596	91	8	by	by	ADP
eurjchem-1596	91	9	comparing	compare	VERB
eurjchem-1596	91	10	stability	stability	NOUN
eurjchem-1596	91	11	samples	sample	NOUN
eurjchem-1596	91	12	against	against	ADP
eurjchem-1596	91	13	freshly	freshly	ADV
eurjchem-1596	91	14	prepared	prepare	VERB
eurjchem-1596	91	15	calibration	calibration	NOUN
eurjchem-1596	91	16	samples	sample	NOUN
eurjchem-1596	91	17	.	.	PUNCT
eurjchem-1596	92	1	the	the	DET
eurjchem-1596	92	2	stability	stability	NOUN
eurjchem-1596	92	3	experiments	experiment	NOUN
eurjchem-1596	92	4	in	in	ADP
eurjchem-1596	92	5	plasma	plasma	NOUN
eurjchem-1596	92	6	were	be	AUX
eurjchem-1596	92	7	considered	consider	VERB
eurjchem-1596	92	8	stable	stable	ADJ
eurjchem-1596	92	9	,	,	PUNCT
eurjchem-1596	92	10	if	if	SCONJ
eurjchem-1596	92	11	the	the	DET
eurjchem-1596	92	12	deviation	deviation	NOUN
eurjchem-1596	92	13	from	from	ADP
eurjchem-1596	92	14	nominal	nominal	ADJ
eurjchem-1596	92	15	value	value	NOUN
eurjchem-1596	92	16	(	(	PUNCT
eurjchem-1596	92	17	±15	±15	NOUN
eurjchem-1596	92	18	%	%	NOUN
eurjchem-1596	92	19	)	)	PUNCT
eurjchem-1596	92	20	and	and	CCONJ
eurjchem-1596	92	21	precision	precision	NOUN
eurjchem-1596	92	22	(	(	PUNCT
eurjchem-1596	92	23	cv	cv	PROPN
eurjchem-1596	92	24	≤	≤	NUM
eurjchem-1596	92	25	15	15	NUM
eurjchem-1596	92	26	%	%	NOUN
eurjchem-1596	92	27	)	)	PUNCT
eurjchem-1596	92	28	were	be	AUX
eurjchem-1596	92	29	within	within	ADP
eurjchem-1596	92	30	the	the	DET
eurjchem-1596	92	31	acceptable	acceptable	ADJ
eurjchem-1596	92	32	limits	limit	NOUN
eurjchem-1596	92	33	.	.	PUNCT
eurjchem-1596	93	1	prepared	prepare	VERB
eurjchem-1596	93	2	stock	stock	NOUN
eurjchem-1596	93	3	solutions	solution	NOUN
eurjchem-1596	93	4	and	and	CCONJ
eurjchem-1596	93	5	working	working	NOUN
eurjchem-1596	93	6	dilutions	dilution	NOUN
eurjchem-1596	93	7	were	be	AUX
eurjchem-1596	93	8	considered	consider	VERB
eurjchem-1596	93	9	stable	stable	ADJ
eurjchem-1596	93	10	if	if	SCONJ
eurjchem-1596	93	11	deviation	deviation	NOUN
eurjchem-1596	93	12	between	between	ADP
eurjchem-1596	93	13	stability	stability	NOUN
eurjchem-1596	93	14	and	and	CCONJ
eurjchem-1596	93	15	comparison	comparison	NOUN
eurjchem-1596	93	16	(	(	PUNCT
eurjchem-1596	93	17	freshly	freshly	ADV
eurjchem-1596	93	18	prepared	prepare	VERB
eurjchem-1596	93	19	)	)	PUNCT
eurjchem-1596	93	20	were	be	AUX
eurjchem-1596	93	21	within	within	ADP
eurjchem-1596	93	22	±10	±10	NOUN
eurjchem-1596	93	23	%	%	NOUN
eurjchem-1596	93	24	.	.	PUNCT
eurjchem-1596	94	1	3.2.1	3.2.1	NUM
eurjchem-1596	94	2	.	.	PUNCT
eurjchem-1596	94	3	carryover	carryover	NOUN
eurjchem-1596	94	4	and	and	CCONJ
eurjchem-1596	94	5	cleaning	clean	VERB
eurjchem-1596	94	6	validation	validation	NOUN
eurjchem-1596	94	7	extracted	extract	VERB
eurjchem-1596	94	8	blank	blank	ADJ
eurjchem-1596	94	9	,	,	PUNCT
eurjchem-1596	94	10	high	high	ADJ
eurjchem-1596	94	11	standard	standard	NOUN
eurjchem-1596	94	12	followed	follow	VERB
eurjchem-1596	94	13	by	by	ADP
eurjchem-1596	94	14	two	two	NUM
eurjchem-1596	94	15	extracted	extract	VERB
eurjchem-1596	94	16	blank	blank	ADJ
eurjchem-1596	94	17	samples	sample	NOUN
eurjchem-1596	94	18	and	and	CCONJ
eurjchem-1596	94	19	low	low	ADJ
eurjchem-1596	94	20	standard	standard	ADJ
eurjchem-1596	94	21	sample	sample	NOUN
eurjchem-1596	94	22	were	be	AUX
eurjchem-1596	94	23	injected	inject	VERB
eurjchem-1596	94	24	to	to	PART
eurjchem-1596	94	25	check	check	VERB
eurjchem-1596	94	26	the	the	DET
eurjchem-1596	94	27	carryover	carryover	NOUN
eurjchem-1596	94	28	test	test	NOUN
eurjchem-1596	94	29	.	.	PUNCT
eurjchem-1596	95	1	carryover	carryover	NOUN
eurjchem-1596	95	2	should	should	AUX
eurjchem-1596	95	3	n’t	not	PART
eurjchem-1596	95	4	be	be	AUX
eurjchem-1596	95	5	more	more	ADJ
eurjchem-1596	95	6	than	than	ADP
eurjchem-1596	95	7	20	20	NUM
eurjchem-1596	95	8	%	%	NOUN
eurjchem-1596	95	9	and	and	CCONJ
eurjchem-1596	95	10	5	5	NUM
eurjchem-1596	95	11	%	%	NOUN
eurjchem-1596	95	12	at	at	ADP
eurjchem-1596	95	13	retention	retention	NOUN
eurjchem-1596	95	14	time	time	NOUN
eurjchem-1596	95	15	of	of	ADP
eurjchem-1596	95	16	analyte	analyte	NOUN
eurjchem-1596	95	17	and	and	CCONJ
eurjchem-1596	95	18	internal	internal	ADJ
eurjchem-1596	95	19	standard	standard	NOUN
eurjchem-1596	95	20	respectively	respectively	ADV
eurjchem-1596	95	21	.	.	PUNCT
eurjchem-1596	96	1	all	all	DET
eurjchem-1596	96	2	the	the	DET
eurjchem-1596	96	3	glassware	glassware	NOUN
eurjchem-1596	96	4	used	use	VERB
eurjchem-1596	96	5	in	in	ADP
eurjchem-1596	96	6	the	the	DET
eurjchem-1596	96	7	study	study	NOUN
eurjchem-1596	96	8	was	be	AUX
eurjchem-1596	96	9	washed	wash	VERB
eurjchem-1596	96	10	with	with	ADP
eurjchem-1596	96	11	diluent	diluent	NOUN
eurjchem-1596	96	12	and	and	CCONJ
eurjchem-1596	96	13	injected	inject	VERB
eurjchem-1596	96	14	into	into	ADP
eurjchem-1596	96	15	the	the	DET
eurjchem-1596	96	16	system	system	NOUN
eurjchem-1596	96	17	with	with	ADP
eurjchem-1596	96	18	method	method	NOUN
eurjchem-1596	96	19	conditions	condition	NOUN
eurjchem-1596	96	20	to	to	PART
eurjchem-1596	96	21	check	check	VERB
eurjchem-1596	96	22	the	the	DET
eurjchem-1596	96	23	presence	presence	NOUN
eurjchem-1596	96	24	of	of	ADP
eurjchem-1596	96	25	potential	potential	ADJ
eurjchem-1596	96	26	interferences	interference	NOUN
eurjchem-1596	96	27	from	from	ADP
eurjchem-1596	96	28	glassware	glassware	NOUN
eurjchem-1596	96	29	materials	material	NOUN
eurjchem-1596	96	30	.	.	PUNCT
eurjchem-1596	97	1	3.2.2	3.2.2	NUM
eurjchem-1596	97	2	.	.	PUNCT
eurjchem-1596	97	3	selectivity	selectivity	NOUN
eurjchem-1596	97	4	the	the	DET
eurjchem-1596	97	5	selectivity	selectivity	NOUN
eurjchem-1596	97	6	of	of	ADP
eurjchem-1596	97	7	the	the	DET
eurjchem-1596	97	8	method	method	NOUN
eurjchem-1596	97	9	was	be	AUX
eurjchem-1596	97	10	determined	determine	VERB
eurjchem-1596	97	11	to	to	PART
eurjchem-1596	97	12	check	check	VERB
eurjchem-1596	97	13	the	the	DET
eurjchem-1596	97	14	potential	potential	ADJ
eurjchem-1596	97	15	interferences	interference	NOUN
eurjchem-1596	97	16	of	of	ADP
eurjchem-1596	97	17	endogenous	endogenous	ADJ
eurjchem-1596	97	18	compounds	compound	NOUN
eurjchem-1596	97	19	present	present	ADJ
eurjchem-1596	97	20	in	in	ADP
eurjchem-1596	97	21	biological	biological	ADJ
eurjchem-1596	97	22	matrix	matrix	NOUN
eurjchem-1596	97	23	or	or	CCONJ
eurjchem-1596	97	24	co‐eluting	co‐eluting	NOUN
eurjchem-1596	97	25	interferences	interference	NOUN
eurjchem-1596	97	26	at	at	ADP
eurjchem-1596	97	27	the	the	DET
eurjchem-1596	97	28	retention	retention	NOUN
eurjchem-1596	97	29	time	time	NOUN
eurjchem-1596	97	30	of	of	ADP
eurjchem-1596	97	31	the	the	DET
eurjchem-1596	97	32	analyte	analyte	NOUN
eurjchem-1596	97	33	and	and	CCONJ
eurjchem-1596	97	34	istd	istd	NOUN
eurjchem-1596	97	35	.	.	PUNCT
eurjchem-1596	98	1	total	total	NOUN
eurjchem-1596	98	2	of	of	ADP
eurjchem-1596	98	3	12	12	NUM
eurjchem-1596	98	4	human	human	ADJ
eurjchem-1596	98	5	blank	blank	ADJ
eurjchem-1596	98	6	plasma	plasma	NOUN
eurjchem-1596	98	7	samples	sample	NOUN
eurjchem-1596	98	8	were	be	AUX
eurjchem-1596	98	9	processed	process	VERB
eurjchem-1596	98	10	as	as	ADP
eurjchem-1596	98	11	per	per	ADP
eurjchem-1596	98	12	sample	sample	NOUN
eurjchem-1596	98	13	extraction	extraction	NOUN
eurjchem-1596	98	14	procedure	procedure	NOUN
eurjchem-1596	98	15	as	as	SCONJ
eurjchem-1596	98	16	follows	follow	VERB
eurjchem-1596	98	17	:	:	PUNCT
eurjchem-1596	98	18	8	8	NUM
eurjchem-1596	98	19	normal	normal	ADJ
eurjchem-1596	98	20	,	,	PUNCT
eurjchem-1596	98	21	2	2	NUM
eurjchem-1596	98	22	lipemic	lipemic	NOUN
eurjchem-1596	98	23	and	and	CCONJ
eurjchem-1596	98	24	2	2	NUM
eurjchem-1596	98	25	heamolytic	heamolytic	ADJ
eurjchem-1596	98	26	plasma	plasma	NOUN
eurjchem-1596	98	27	lots	lot	NOUN
eurjchem-1596	98	28	.	.	PUNCT
eurjchem-1596	99	1	no	no	DET
eurjchem-1596	99	2	interference	interference	NOUN
eurjchem-1596	99	3	peaks	peak	NOUN
eurjchem-1596	99	4	were	be	AUX
eurjchem-1596	99	5	observed	observe	VERB
eurjchem-1596	99	6	at	at	ADP
eurjchem-1596	99	7	the	the	DET
eurjchem-1596	99	8	retention	retention	NOUN
eurjchem-1596	99	9	time	time	NOUN
eurjchem-1596	99	10	of	of	ADP
eurjchem-1596	99	11	analyte	analyte	NOUN
eurjchem-1596	99	12	and	and	CCONJ
eurjchem-1596	99	13	istd	istd	NOUN
eurjchem-1596	99	14	.	.	PUNCT
eurjchem-1596	100	1	identical	identical	ADJ
eurjchem-1596	100	2	chromatograms	chromatogram	NOUN
eurjchem-1596	100	3	of	of	ADP
eurjchem-1596	100	4	plasma	plasma	NOUN
eurjchem-1596	100	5	lots	lot	NOUN
eurjchem-1596	100	6	prove	prove	VERB
eurjchem-1596	100	7	assay	assay	ADJ
eurjchem-1596	100	8	diversity	diversity	NOUN
eurjchem-1596	100	9	.	.	PUNCT
eurjchem-1596	101	1	3.2.3	3.2.3	X
eurjchem-1596	101	2	.	.	X
eurjchem-1596	101	3	matrix	matrix	NOUN
eurjchem-1596	101	4	effect	effect	NOUN
eurjchem-1596	101	5	3.2.3.1	3.2.3.1	PROPN
eurjchem-1596	101	6	.	.	PROPN
eurjchem-1596	101	7	is	be	AUX
eurjchem-1596	101	8	normalized	normalize	VERB
eurjchem-1596	101	9	factor	factor	NOUN
eurjchem-1596	101	10	and	and	CCONJ
eurjchem-1596	101	11	direct	direct	ADJ
eurjchem-1596	101	12	quantification	quantification	NOUN
eurjchem-1596	101	13	the	the	DET
eurjchem-1596	101	14	effect	effect	NOUN
eurjchem-1596	101	15	of	of	ADP
eurjchem-1596	101	16	the	the	DET
eurjchem-1596	101	17	presence	presence	NOUN
eurjchem-1596	101	18	of	of	ADP
eurjchem-1596	101	19	endogenous	endogenous	ADJ
eurjchem-1596	101	20	matrix	matrix	NOUN
eurjchem-1596	101	21	components	component	NOUN
eurjchem-1596	101	22	on	on	ADP
eurjchem-1596	101	23	ulipristal	ulipristal	ADJ
eurjchem-1596	101	24	acetate	acetate	NOUN
eurjchem-1596	101	25	was	be	AUX
eurjchem-1596	101	26	evaluated	evaluate	VERB
eurjchem-1596	101	27	in	in	ADP
eurjchem-1596	101	28	10	10	NUM
eurjchem-1596	101	29	different	different	ADJ
eurjchem-1596	101	30	screened	screen	VERB
eurjchem-1596	101	31	blank	blank	ADJ
eurjchem-1596	101	32	plasma	plasma	NOUN
eurjchem-1596	101	33	lots	lot	NOUN
eurjchem-1596	101	34	(	(	PUNCT
eurjchem-1596	101	35	6	6	NUM
eurjchem-1596	101	36	normal	normal	ADJ
eurjchem-1596	101	37	,	,	PUNCT
eurjchem-1596	101	38	2	2	NUM
eurjchem-1596	101	39	lipemic	lipemic	NOUN
eurjchem-1596	101	40	and	and	CCONJ
eurjchem-1596	101	41	2	2	NUM
eurjchem-1596	101	42	hemolytic	hemolytic	NOUN
eurjchem-1596	101	43	)	)	PUNCT
eurjchem-1596	101	44	containing	contain	VERB
eurjchem-1596	101	45	k2edta	k2edta	NOUN
eurjchem-1596	101	46	as	as	ADP
eurjchem-1596	101	47	an	an	DET
eurjchem-1596	101	48	anticoagulant	anticoagulant	NOUN
eurjchem-1596	101	49	.	.	PUNCT
eurjchem-1596	102	1	from	from	ADP
eurjchem-1596	102	2	each	each	DET
eurjchem-1596	102	3	plasma	plasma	NOUN
eurjchem-1596	102	4	lot	lot	NOUN
eurjchem-1596	102	5	a	a	DET
eurjchem-1596	102	6	total	total	NOUN
eurjchem-1596	102	7	of	of	ADP
eurjchem-1596	102	8	6	6	NUM
eurjchem-1596	102	9	samples	sample	NOUN
eurjchem-1596	102	10	(	(	PUNCT
eurjchem-1596	102	11	three	three	NUM
eurjchem-1596	102	12	replicates	replicate	NOUN
eurjchem-1596	102	13	each	each	PRON
eurjchem-1596	102	14	for	for	ADP
eurjchem-1596	102	15	lqc	lqc	NOUN
eurjchem-1596	102	16	and	and	CCONJ
eurjchem-1596	102	17	hqc	hqc	PROPN
eurjchem-1596	102	18	)	)	PUNCT
eurjchem-1596	102	19	are	be	AUX
eurjchem-1596	102	20	processed	process	VERB
eurjchem-1596	102	21	and	and	CCONJ
eurjchem-1596	102	22	injected	inject	VERB
eurjchem-1596	102	23	.	.	PUNCT
eurjchem-1596	103	1	all	all	DET
eurjchem-1596	103	2	back	back	ADV
eurjchem-1596	103	3	calculated	calculate	VERB
eurjchem-1596	103	4	concentrations	concentration	NOUN
eurjchem-1596	103	5	their	their	PRON
eurjchem-1596	103	6	average	average	ADJ
eurjchem-1596	103	7	and	and	CCONJ
eurjchem-1596	103	8	individual	individual	ADJ
eurjchem-1596	103	9	at	at	ADP
eurjchem-1596	103	10	lqc	lqc	PROPN
eurjchem-1596	103	11	,	,	PUNCT
eurjchem-1596	103	12	hqc	hqc	PROPN
eurjchem-1596	103	13	were	be	AUX
eurjchem-1596	103	14	within	within	ADP
eurjchem-1596	103	15	±15	±15	NOUN
eurjchem-1596	103	16	%	%	NOUN
eurjchem-1596	103	17	.	.	PUNCT
eurjchem-1596	104	1	each	each	DET
eurjchem-1596	104	2	two	two	NUM
eurjchem-1596	104	3	samples	sample	NOUN
eurjchem-1596	104	4	were	be	AUX
eurjchem-1596	104	5	processed	process	VERB
eurjchem-1596	104	6	from	from	ADP
eurjchem-1596	104	7	each	each	DET
eurjchem-1596	104	8	blank	blank	ADJ
eurjchem-1596	104	9	plasma	plasma	NOUN
eurjchem-1596	104	10	lot	lot	NOUN
eurjchem-1596	104	11	.	.	PUNCT
eurjchem-1596	105	1	samples	sample	NOUN
eurjchem-1596	105	2	were	be	AUX
eurjchem-1596	105	3	reconstituted	reconstitute	VERB
eurjchem-1596	105	4	with	with	ADP
eurjchem-1596	105	5	respective	respective	ADJ
eurjchem-1596	105	6	solutions	solution	NOUN
eurjchem-1596	105	7	(	(	PUNCT
eurjchem-1596	105	8	post	post	NOUN
eurjchem-1596	105	9	spiking	spiking	ADJ
eurjchem-1596	105	10	,	,	PUNCT
eurjchem-1596	105	11	one	one	NUM
eurjchem-1596	105	12	lqc	lqc	NOUN
eurjchem-1596	105	13	and	and	CCONJ
eurjchem-1596	105	14	one	one	NUM
eurjchem-1596	105	15	hqc	hqc	NOUN
eurjchem-1596	105	16	)	)	PUNCT
eurjchem-1596	105	17	prepared	prepare	VERB
eurjchem-1596	105	18	in	in	ADP
eurjchem-1596	105	19	mobile	mobile	ADJ
eurjchem-1596	105	20	phase	phase	NOUN
eurjchem-1596	105	21	to	to	PART
eurjchem-1596	105	22	get	get	VERB
eurjchem-1596	105	23	the	the	DET
eurjchem-1596	105	24	equal	equal	ADJ
eurjchem-1596	105	25	concentration	concentration	NOUN
eurjchem-1596	105	26	as	as	ADP
eurjchem-1596	105	27	extracted	extract	VERB
eurjchem-1596	105	28	samples	sample	NOUN
eurjchem-1596	105	29	.	.	PUNCT
eurjchem-1596	106	1	prepare	prepare	VERB
eurjchem-1596	106	2	aqueous	aqueous	ADJ
eurjchem-1596	106	3	samples	sample	NOUN
eurjchem-1596	106	4	of	of	ADP
eurjchem-1596	106	5	lqc	lqc	NOUN
eurjchem-1596	106	6	and	and	CCONJ
eurjchem-1596	106	7	hqc	hqc	INTJ
eurjchem-1596	106	8	having	have	VERB
eurjchem-1596	106	9	the	the	DET
eurjchem-1596	106	10	concentration	concentration	NOUN
eurjchem-1596	106	11	equal	equal	ADJ
eurjchem-1596	106	12	to	to	ADP
eurjchem-1596	106	13	the	the	DET
eurjchem-1596	106	14	post	post	NOUN
eurjchem-1596	106	15	spiked	spiked	ADJ
eurjchem-1596	106	16	samples	sample	NOUN
eurjchem-1596	106	17	.	.	PUNCT
eurjchem-1596	107	1	the	the	DET
eurjchem-1596	107	2	response	response	NOUN
eurjchem-1596	107	3	ratio	ratio	NOUN
eurjchem-1596	107	4	of	of	ADP
eurjchem-1596	107	5	analyte	analyte	NOUN
eurjchem-1596	107	6	and	and	CCONJ
eurjchem-1596	107	7	istd	istd	NOUN
eurjchem-1596	107	8	in	in	ADP
eurjchem-1596	107	9	the	the	DET
eurjchem-1596	107	10	post	post	NOUN
eurjchem-1596	107	11	spiked	spiked	ADJ
eurjchem-1596	107	12	samples	sample	NOUN
eurjchem-1596	107	13	versus	versus	ADP
eurjchem-1596	107	14	aqueous	aqueous	ADJ
eurjchem-1596	107	15	samples	sample	NOUN
eurjchem-1596	107	16	(	(	PUNCT
eurjchem-1596	107	17	considering	consider	VERB
eurjchem-1596	107	18	100	100	NUM
eurjchem-1596	107	19	%	%	NOUN
eurjchem-1596	107	20	response	response	NOUN
eurjchem-1596	107	21	)	)	PUNCT
eurjchem-1596	107	22	was	be	AUX
eurjchem-1596	107	23	calculated	calculate	VERB
eurjchem-1596	107	24	.	.	PUNCT
eurjchem-1596	108	1	mean	mean	VERB
eurjchem-1596	108	2	response	response	NOUN
eurjchem-1596	108	3	ratio	ratio	NOUN
eurjchem-1596	108	4	(	(	PUNCT
eurjchem-1596	108	5	%	%	INTJ
eurjchem-1596	108	6	)	)	PUNCT
eurjchem-1596	108	7	and	and	CCONJ
eurjchem-1596	108	8	precision	precision	NOUN
eurjchem-1596	108	9	(	(	PUNCT
eurjchem-1596	108	10	%	%	INTJ
eurjchem-1596	108	11	cv	cv	PROPN
eurjchem-1596	108	12	)	)	PUNCT
eurjchem-1596	108	13	of	of	ADP
eurjchem-1596	108	14	the	the	DET
eurjchem-1596	108	15	istd	istd	NOUN
eurjchem-1596	108	16	normalized	normalize	VERB
eurjchem-1596	108	17	matrix	matrix	NOUN
eurjchem-1596	108	18	factor	factor	NOUN
eurjchem-1596	108	19	for	for	ADP
eurjchem-1596	108	20	analyte	analyte	NOUN
eurjchem-1596	108	21	in	in	ADP
eurjchem-1596	108	22	k2edta	k2edta	PROPN
eurjchem-1596	108	23	were	be	AUX
eurjchem-1596	108	24	0.98	0.98	NUM
eurjchem-1596	108	25	and	and	CCONJ
eurjchem-1596	108	26	6.30	6.30	NUM
eurjchem-1596	108	27	for	for	ADP
eurjchem-1596	108	28	lqc	lqc	NOUN
eurjchem-1596	108	29	and	and	CCONJ
eurjchem-1596	108	30	1.01	1.01	NUM
eurjchem-1596	108	31	and	and	CCONJ
eurjchem-1596	108	32	4.80	4.80	NUM
eurjchem-1596	108	33	for	for	ADP
eurjchem-1596	108	34	hqc	hqc	PROPN
eurjchem-1596	108	35	,	,	PUNCT
eurjchem-1596	108	36	shows	show	VERB
eurjchem-1596	108	37	that	that	SCONJ
eurjchem-1596	108	38	there	there	PRON
eurjchem-1596	108	39	is	be	VERB
eurjchem-1596	108	40	negligible	negligible	ADJ
eurjchem-1596	108	41	ion	ion	NOUN
eurjchem-1596	108	42	suppression	suppression	NOUN
eurjchem-1596	108	43	or	or	CCONJ
eurjchem-1596	108	44	enhancement	enhancement	NOUN
eurjchem-1596	108	45	.	.	PUNCT
eurjchem-1596	109	1	the	the	DET
eurjchem-1596	109	2	results	result	NOUN
eurjchem-1596	109	3	were	be	AUX
eurjchem-1596	109	4	shown	show	VERB
eurjchem-1596	109	5	in	in	ADP
eurjchem-1596	109	6	table	table	NOUN
eurjchem-1596	109	7	1	1	NUM
eurjchem-1596	109	8	.	.	PUNCT
eurjchem-1596	110	1	pappula	pappula	PROPN
eurjchem-1596	110	2	et	et	PROPN
eurjchem-1596	110	3	al	al	PROPN
eurjchem-1596	110	4	.	.	PUNCT
eurjchem-1596	110	5	/	/	SYM
eurjchem-1596	110	6	european	european	PROPN
eurjchem-1596	110	7	journal	journal	PROPN
eurjchem-1596	110	8	of	of	ADP
eurjchem-1596	110	9	chemistry	chemistry	NOUN
eurjchem-1596	110	10	8	8	NUM
eurjchem-1596	110	11	(	(	PUNCT
eurjchem-1596	110	12	3	3	NUM
eurjchem-1596	110	13	)	)	PUNCT
eurjchem-1596	110	14	(	(	PUNCT
eurjchem-1596	110	15	2017	2017	NUM
eurjchem-1596	110	16	)	)	PUNCT
eurjchem-1596	110	17	258‐264	258‐264	NOUN
eurjchem-1596	110	18	261	261	NUM
eurjchem-1596	110	19	table	table	NOUN
eurjchem-1596	110	20	1	1	NUM
eurjchem-1596	110	21	.	.	PUNCT
eurjchem-1596	110	22	matrix	matrix	NOUN
eurjchem-1596	110	23	effect	effect	NOUN
eurjchem-1596	110	24	data	datum	NOUN
eurjchem-1596	110	25	results	result	NOUN
eurjchem-1596	110	26	,	,	PUNCT
eurjchem-1596	110	27	mf‐matrix	mf‐matrix	ADJ
eurjchem-1596	110	28	factor	factor	NOUN
eurjchem-1596	110	29	,	,	PUNCT
eurjchem-1596	110	30	isnmf‐internal	isnmf‐internal	ADJ
eurjchem-1596	110	31	standard	standard	NOUN
eurjchem-1596	110	32	normalised	normalise	VERB
eurjchem-1596	110	33	factor	factor	NOUN
eurjchem-1596	110	34	.	.	PUNCT
eurjchem-1596	111	1	blank	blank	ADJ
eurjchem-1596	111	2	plasma	plasma	NOUN
eurjchem-1596	111	3	lots	lot	NOUN
eurjchem-1596	111	4	lqc	lqc	VERB
eurjchem-1596	111	5	hqc	hqc	INTJ
eurjchem-1596	111	6	mf	mf	NOUN
eurjchem-1596	111	7	analyte	analyte	NOUN
eurjchem-1596	111	8	mf	mf	NOUN
eurjchem-1596	111	9	istd	istd	PROPN
eurjchem-1596	111	10	isnmf	isnmf	NOUN
eurjchem-1596	111	11	mf	mf	PUNCT
eurjchem-1596	111	12	analyte	analyte	NOUN
eurjchem-1596	111	13	mf	mf	VERB
eurjchem-1596	111	14	istd	istd	NOUN
eurjchem-1596	111	15	isnmf	isnmf	NOUN
eurjchem-1596	111	16	lot‐1	lot‐1	PROPN
eurjchem-1596	111	17	0.91	0.91	NUM
eurjchem-1596	111	18	0.92	0.92	NUM
eurjchem-1596	111	19	0.99	0.99	NUM
eurjchem-1596	111	20	0.94	0.94	NUM
eurjchem-1596	111	21	0.88	0.88	NUM
eurjchem-1596	111	22	1.07	1.07	NUM
eurjchem-1596	111	23	lot‐2	lot‐2	PROPN
eurjchem-1596	111	24	0.88	0.88	NUM
eurjchem-1596	111	25	0.95	0.95	NUM
eurjchem-1596	111	26	0.93	0.93	NUM
eurjchem-1596	111	27	0.88	0.88	NUM
eurjchem-1596	111	28	0.84	0.84	NUM
eurjchem-1596	111	29	1.05	1.05	NUM
eurjchem-1596	111	30	lot‐3	lot‐3	NOUN
eurjchem-1596	111	31	0.85	0.85	NUM
eurjchem-1596	111	32	0.91	0.91	NUM
eurjchem-1596	111	33	0.93	0.93	NUM
eurjchem-1596	111	34	0.92	0.92	NUM
eurjchem-1596	111	35	0.89	0.89	NUM
eurjchem-1596	111	36	1.03	1.03	NUM
eurjchem-1596	111	37	lot‐4	lot‐4	PROPN
eurjchem-1596	111	38	0.86	0.86	NUM
eurjchem-1596	111	39	0.92	0.92	NUM
eurjchem-1596	111	40	0.93	0.93	NUM
eurjchem-1596	111	41	0.93	0.93	NUM
eurjchem-1596	111	42	0.96	0.96	NUM
eurjchem-1596	111	43	0.97	0.97	NUM
eurjchem-1596	111	44	lot‐5	lot‐5	ADP
eurjchem-1596	111	45	0.92	0.92	NUM
eurjchem-1596	111	46	0.98	0.98	NUM
eurjchem-1596	111	47	0.94	0.94	NUM
eurjchem-1596	111	48	0.94	0.94	NUM
eurjchem-1596	111	49	0.89	0.89	NUM
eurjchem-1596	111	50	1.06	1.06	NUM
eurjchem-1596	111	51	lot‐6	lot‐6	NOUN
eurjchem-1596	111	52	0.91	0.91	NUM
eurjchem-1596	111	53	0.86	0.86	NUM
eurjchem-1596	111	54	1.06	1.06	NUM
eurjchem-1596	111	55	0.92	0.92	NUM
eurjchem-1596	111	56	0.95	0.95	NUM
eurjchem-1596	111	57	0.97	0.97	NUM
eurjchem-1596	111	58	lot‐7	lot‐7	PROPN
eurjchem-1596	111	59	hemolytic	hemolytic	VERB
eurjchem-1596	111	60	0.92	0.92	NUM
eurjchem-1596	111	61	0.85	0.85	NUM
eurjchem-1596	111	62	1.08	1.08	NUM
eurjchem-1596	111	63	0.88	0.88	NUM
eurjchem-1596	111	64	0.94	0.94	NUM
eurjchem-1596	111	65	0.94	0.94	NUM
eurjchem-1596	111	66	lot‐8	lot‐8	NOUN
eurjchem-1596	111	67	hemolytic	hemolytic	ADJ
eurjchem-1596	111	68	0.86	0.86	NUM
eurjchem-1596	111	69	0.88	0.88	NUM
eurjchem-1596	111	70	0.98	0.98	NUM
eurjchem-1596	111	71	0.86	0.86	NUM
eurjchem-1596	111	72	0.82	0.82	NUM
eurjchem-1596	111	73	1.05	1.05	NUM
eurjchem-1596	111	74	lot‐9	lot‐9	ADJ
eurjchem-1596	111	75	lipemic	lipemic	NOUN
eurjchem-1596	111	76	0.89	0.89	NUM
eurjchem-1596	111	77	0.94	0.94	NUM
eurjchem-1596	111	78	0.95	0.95	NUM
eurjchem-1596	111	79	0.92	0.92	NUM
eurjchem-1596	111	80	0.88	0.88	NUM
eurjchem-1596	111	81	1.05	1.05	NUM
eurjchem-1596	111	82	lot‐10	lot‐10	NOUN
eurjchem-1596	111	83	lipemic	lipemic	NOUN
eurjchem-1596	111	84	0.91	0.91	NUM
eurjchem-1596	111	85	0.85	0.85	NUM
eurjchem-1596	111	86	1.07	1.07	NUM
eurjchem-1596	111	87	0.92	0.92	NUM
eurjchem-1596	111	88	0.96	0.96	NUM
eurjchem-1596	111	89	0.96	0.96	NUM
eurjchem-1596	111	90	mean	mean	NOUN
eurjchem-1596	111	91	0.9860	0.9860	NUM
eurjchem-1596	111	92	mean	mean	NOUN
eurjchem-1596	111	93	1.013	1.013	NUM
eurjchem-1596	111	94	sd	sd	NOUN
eurjchem-1596	111	95	(	(	PUNCT
eurjchem-1596	111	96	standard	standard	ADJ
eurjchem-1596	111	97	deviation	deviation	NOUN
eurjchem-1596	111	98	)	)	PUNCT
eurjchem-1596	111	99	0.0618	0.0618	NUM
eurjchem-1596	111	100	sd	sd	ADP
eurjchem-1596	111	101	0.0491	0.0491	NUM
eurjchem-1596	111	102	%	%	NOUN
eurjchem-1596	111	103	cv	cv	PROPN
eurjchem-1596	111	104	(	(	PUNCT
eurjchem-1596	111	105	coefficient	coefficient	NOUN
eurjchem-1596	111	106	of	of	ADP
eurjchem-1596	111	107	variation	variation	NOUN
eurjchem-1596	111	108	)	)	PUNCT
eurjchem-1596	111	109	6.30	6.30	NUM
eurjchem-1596	111	110	%	%	NOUN
eurjchem-1596	111	111	cv	cv	NOUN
eurjchem-1596	111	112	4.80	4.80	NUM
eurjchem-1596	111	113	table	table	NOUN
eurjchem-1596	111	114	2	2	NUM
eurjchem-1596	111	115	.	.	PUNCT
eurjchem-1596	111	116	typical	typical	ADJ
eurjchem-1596	111	117	extraction	extraction	NOUN
eurjchem-1596	111	118	recoveries	recovery	NOUN
eurjchem-1596	111	119	of	of	ADP
eurjchem-1596	111	120	analyte	analyte	NOUN
eurjchem-1596	111	121	and	and	CCONJ
eurjchem-1596	111	122	istd	istd	NOUN
eurjchem-1596	111	123	from	from	ADP
eurjchem-1596	111	124	solvents	solvent	NOUN
eurjchem-1596	111	125	and	and	CCONJ
eurjchem-1596	111	126	solvent	solvent	ADJ
eurjchem-1596	111	127	mixtures	mixture	NOUN
eurjchem-1596	111	128	.	.	PUNCT
eurjchem-1596	112	1	extraction	extraction	NOUN
eurjchem-1596	112	2	solvent	solvent	NOUN
eurjchem-1596	112	3	/	/	SYM
eurjchem-1596	112	4	mixture	mixture	NOUN
eurjchem-1596	112	5	%	%	NOUN
eurjchem-1596	112	6	average	average	ADJ
eurjchem-1596	112	7	recovery	recovery	NOUN
eurjchem-1596	112	8	of	of	ADP
eurjchem-1596	112	9	analyte	analyte	NOUN
eurjchem-1596	112	10	%	%	NOUN
eurjchem-1596	112	11	recovery	recovery	NOUN
eurjchem-1596	112	12	of	of	ADP
eurjchem-1596	112	13	istd	istd	NOUN
eurjchem-1596	112	14	methyl	methyl	NOUN
eurjchem-1596	112	15	tert‐butyl	tert‐butyl	ADP
eurjchem-1596	112	16	ether	ether	NOUN
eurjchem-1596	112	17	(	(	PUNCT
eurjchem-1596	112	18	mtbe	mtbe	NOUN
eurjchem-1596	112	19	)	)	PUNCT
eurjchem-1596	112	20	45.5	45.5	NUM
eurjchem-1596	112	21	38.2	38.2	NUM
eurjchem-1596	112	22	di	di	PROPN
eurjchem-1596	112	23	ethyl	ethyl	PROPN
eurjchem-1596	112	24	ether	ether	PROPN
eurjchem-1596	112	25	(	(	PUNCT
eurjchem-1596	112	26	dee	dee	PROPN
eurjchem-1596	112	27	)	)	PUNCT
eurjchem-1596	112	28	51.0	51.0	NUM
eurjchem-1596	112	29	65.0	65.0	NUM
eurjchem-1596	112	30	mtbe	mtbe	NOUN
eurjchem-1596	112	31	:	:	PUNCT
eurjchem-1596	112	32	dee	dee	PROPN
eurjchem-1596	112	33	(	(	PUNCT
eurjchem-1596	112	34	70:30	70:30	NUM
eurjchem-1596	112	35	,	,	PUNCT
eurjchem-1596	112	36	v	v	NOUN
eurjchem-1596	112	37	:	:	SYM
eurjchem-1596	112	38	v	v	NOUN
eurjchem-1596	112	39	)	)	PUNCT
eurjchem-1596	112	40	61.0	61.0	NUM
eurjchem-1596	112	41	74.0	74.0	NUM
eurjchem-1596	112	42	mtbe	mtbe	NOUN
eurjchem-1596	112	43	:	:	PUNCT
eurjchem-1596	112	44	ethyl	ethyl	PROPN
eurjchem-1596	112	45	acetate	acetate	PROPN
eurjchem-1596	112	46	(	(	PUNCT
eurjchem-1596	112	47	50:50	50:50	NUM
eurjchem-1596	112	48	,	,	PUNCT
eurjchem-1596	112	49	v	v	NOUN
eurjchem-1596	112	50	:	:	PUNCT
eurjchem-1596	112	51	v	v	NOUN
eurjchem-1596	112	52	)	)	PUNCT
eurjchem-1596	112	53	58.0	58.0	NUM
eurjchem-1596	112	54	63.0	63.0	NUM
eurjchem-1596	112	55	mtbe	mtbe	NOUN
eurjchem-1596	112	56	:	:	PUNCT
eurjchem-1596	112	57	n‐hexane	n‐hexane	X
eurjchem-1596	112	58	(	(	PUNCT
eurjchem-1596	112	59	50:50	50:50	NUM
eurjchem-1596	112	60	,	,	PUNCT
eurjchem-1596	112	61	v	v	NOUN
eurjchem-1596	112	62	:	:	PUNCT
eurjchem-1596	112	63	v	v	NOUN
eurjchem-1596	112	64	)	)	PUNCT
eurjchem-1596	112	65	63.0	63.0	NUM
eurjchem-1596	112	66	64.5	64.5	NUM
eurjchem-1596	112	67	figure	figure	NOUN
eurjchem-1596	112	68	2	2	NUM
eurjchem-1596	112	69	.	.	X
eurjchem-1596	112	70	chromatogram	chromatogram	VERB
eurjchem-1596	112	71	for	for	ADP
eurjchem-1596	112	72	phospholipid	phospholipid	NOUN
eurjchem-1596	112	73	elution	elution	NOUN
eurjchem-1596	112	74	and	and	CCONJ
eurjchem-1596	112	75	long	long	ADJ
eurjchem-1596	112	76	runs	run	NOUN
eurjchem-1596	112	77	.	.	PUNCT
eurjchem-1596	113	1	3.2.3.2	3.2.3.2	X
eurjchem-1596	113	2	.	.	PUNCT
eurjchem-1596	113	3	direct	direct	ADJ
eurjchem-1596	113	4	infusion	infusion	NOUN
eurjchem-1596	113	5	method	method	NOUN
eurjchem-1596	113	6	while	while	SCONJ
eurjchem-1596	113	7	infusing	infuse	VERB
eurjchem-1596	113	8	continues	continue	VERB
eurjchem-1596	113	9	extracted	extract	VERB
eurjchem-1596	113	10	solution	solution	NOUN
eurjchem-1596	113	11	from	from	ADP
eurjchem-1596	113	12	blank	blank	ADJ
eurjchem-1596	113	13	matrix	matrix	NOUN
eurjchem-1596	113	14	,	,	PUNCT
eurjchem-1596	113	15	the	the	DET
eurjchem-1596	113	16	aqueous	aqueous	ADJ
eurjchem-1596	113	17	solution	solution	NOUN
eurjchem-1596	113	18	of	of	ADP
eurjchem-1596	113	19	analyte	analyte	NOUN
eurjchem-1596	113	20	at	at	ADP
eurjchem-1596	113	21	loq	loq	PROPN
eurjchem-1596	113	22	level	level	NOUN
eurjchem-1596	113	23	was	be	AUX
eurjchem-1596	113	24	injected	inject	VERB
eurjchem-1596	113	25	to	to	PART
eurjchem-1596	113	26	check	check	VERB
eurjchem-1596	113	27	the	the	DET
eurjchem-1596	113	28	effect	effect	NOUN
eurjchem-1596	113	29	of	of	ADP
eurjchem-1596	113	30	matrix	matrix	NOUN
eurjchem-1596	113	31	ions	ion	NOUN
eurjchem-1596	113	32	on	on	ADP
eurjchem-1596	113	33	intensity	intensity	NOUN
eurjchem-1596	113	34	and	and	CCONJ
eurjchem-1596	113	35	peak	peak	NOUN
eurjchem-1596	113	36	shape	shape	NOUN
eurjchem-1596	113	37	.	.	PUNCT
eurjchem-1596	114	1	there	there	PRON
eurjchem-1596	114	2	was	be	VERB
eurjchem-1596	114	3	no	no	DET
eurjchem-1596	114	4	suppression	suppression	NOUN
eurjchem-1596	114	5	or	or	CCONJ
eurjchem-1596	114	6	enhancement	enhancement	NOUN
eurjchem-1596	114	7	in	in	ADP
eurjchem-1596	114	8	the	the	DET
eurjchem-1596	114	9	signal	signal	NOUN
eurjchem-1596	114	10	was	be	AUX
eurjchem-1596	114	11	observed	observe	VERB
eurjchem-1596	114	12	.	.	PUNCT
eurjchem-1596	115	1	3.2.3.3	3.2.3.3	X
eurjchem-1596	115	2	.	.	PUNCT
eurjchem-1596	115	3	phospholipid	phospholipid	NOUN
eurjchem-1596	115	4	elution	elution	NOUN
eurjchem-1596	115	5	and	and	CCONJ
eurjchem-1596	115	6	long	long	ADJ
eurjchem-1596	115	7	runs	run	NOUN
eurjchem-1596	115	8	phosphoglycerides	phosphoglyceride	NOUN
eurjchem-1596	115	9	,	,	PUNCT
eurjchem-1596	115	10	source	source	NOUN
eurjchem-1596	115	11	of	of	ADP
eurjchem-1596	115	12	phospholipids	phospholipid	NOUN
eurjchem-1596	115	13	,	,	PUNCT
eurjchem-1596	115	14	present	present	ADJ
eurjchem-1596	115	15	in	in	ADP
eurjchem-1596	115	16	the	the	DET
eurjchem-1596	115	17	cell	cell	NOUN
eurjchem-1596	115	18	membrane	membrane	NOUN
eurjchem-1596	115	19	are	be	AUX
eurjchem-1596	115	20	the	the	DET
eurjchem-1596	115	21	major	major	ADJ
eurjchem-1596	115	22	cause	cause	NOUN
eurjchem-1596	115	23	of	of	ADP
eurjchem-1596	115	24	matrix	matrix	NOUN
eurjchem-1596	115	25	effect	effect	NOUN
eurjchem-1596	115	26	in	in	ADP
eurjchem-1596	115	27	bio	bio	PROPN
eurjchem-1596	115	28	analytical	analytical	ADJ
eurjchem-1596	115	29	methods	method	NOUN
eurjchem-1596	115	30	[	[	X
eurjchem-1596	115	31	11,12	11,12	NUM
eurjchem-1596	115	32	]	]	PUNCT
eurjchem-1596	115	33	.	.	PUNCT
eurjchem-1596	116	1	extracted	extract	VERB
eurjchem-1596	116	2	blank	blank	ADJ
eurjchem-1596	116	3	sample	sample	NOUN
eurjchem-1596	116	4	was	be	AUX
eurjchem-1596	116	5	injected	inject	VERB
eurjchem-1596	116	6	using	use	VERB
eurjchem-1596	116	7	mrm	mrm	PROPN
eurjchem-1596	116	8	(	(	PUNCT
eurjchem-1596	116	9	m	m	PROPN
eurjchem-1596	116	10	/	/	SYM
eurjchem-1596	116	11	z	z	PROPN
eurjchem-1596	116	12	184	184	NUM
eurjchem-1596	116	13	→	→	SYM
eurjchem-1596	116	14	m	m	NOUN
eurjchem-1596	116	15	/	/	SYM
eurjchem-1596	116	16	z	z	PROPN
eurjchem-1596	116	17	184	184	NUM
eurjchem-1596	116	18	)	)	PUNCT
eurjchem-1596	116	19	,	,	PUNCT
eurjchem-1596	116	20	the	the	DET
eurjchem-1596	116	21	most	most	ADV
eurjchem-1596	116	22	commonly	commonly	ADV
eurjchem-1596	116	23	selected	select	VERB
eurjchem-1596	116	24	mrm	mrm	PROPN
eurjchem-1596	116	25	to	to	PART
eurjchem-1596	116	26	check	check	VERB
eurjchem-1596	116	27	the	the	DET
eurjchem-1596	116	28	typical	typical	ADJ
eurjchem-1596	116	29	phospholipids	phospholipid	NOUN
eurjchem-1596	116	30	(	(	PUNCT
eurjchem-1596	116	31	2‐lyso	2‐lyso	NOUN
eurjchem-1596	116	32	and	and	CCONJ
eurjchem-1596	116	33	diradyl	diradyl	PROPN
eurjchem-1596	116	34	phosphocholines	phosphocholine	NOUN
eurjchem-1596	116	35	)	)	PUNCT
eurjchem-1596	116	36	elution	elution	NOUN
eurjchem-1596	116	37	.	.	PUNCT
eurjchem-1596	117	1	further	far	ADV
eurjchem-1596	117	2	,	,	PUNCT
eurjchem-1596	117	3	analytical	analytical	ADJ
eurjchem-1596	117	4	run	run	NOUN
eurjchem-1596	117	5	was	be	AUX
eurjchem-1596	117	6	extended	extend	VERB
eurjchem-1596	117	7	to	to	ADP
eurjchem-1596	117	8	10	10	NUM
eurjchem-1596	117	9	min	min	NOUN
eurjchem-1596	117	10	to	to	PART
eurjchem-1596	117	11	check	check	VERB
eurjchem-1596	117	12	long	long	ADJ
eurjchem-1596	117	13	runs	run	NOUN
eurjchem-1596	117	14	and	and	CCONJ
eurjchem-1596	117	15	phospholipid	phospholipid	NOUN
eurjchem-1596	117	16	elution	elution	NOUN
eurjchem-1596	117	17	[	[	X
eurjchem-1596	117	18	12	12	NUM
eurjchem-1596	117	19	]	]	PUNCT
eurjchem-1596	117	20	.	.	PUNCT
eurjchem-1596	118	1	the	the	DET
eurjchem-1596	118	2	chromatogram	chromatogram	NOUN
eurjchem-1596	118	3	represents	represent	VERB
eurjchem-1596	118	4	that	that	SCONJ
eurjchem-1596	118	5	there	there	PRON
eurjchem-1596	118	6	is	be	VERB
eurjchem-1596	118	7	no	no	DET
eurjchem-1596	118	8	elution	elution	NOUN
eurjchem-1596	118	9	of	of	ADP
eurjchem-1596	118	10	phospholipids	phospholipid	NOUN
eurjchem-1596	118	11	at	at	ADP
eurjchem-1596	118	12	the	the	DET
eurjchem-1596	118	13	retention	retention	NOUN
eurjchem-1596	118	14	time	time	NOUN
eurjchem-1596	118	15	of	of	ADP
eurjchem-1596	118	16	analyte	analyte	NOUN
eurjchem-1596	118	17	and	and	CCONJ
eurjchem-1596	118	18	istd	istd	NOUN
eurjchem-1596	118	19	and	and	CCONJ
eurjchem-1596	118	20	also	also	ADV
eurjchem-1596	118	21	in	in	ADP
eurjchem-1596	118	22	continuous	continuous	ADJ
eurjchem-1596	118	23	run	run	NOUN
eurjchem-1596	118	24	which	which	PRON
eurjchem-1596	118	25	represents	represent	VERB
eurjchem-1596	118	26	sample	sample	NOUN
eurjchem-1596	118	27	cleanliness	cleanliness	NOUN
eurjchem-1596	118	28	.	.	PUNCT
eurjchem-1596	119	1	the	the	DET
eurjchem-1596	119	2	representative	representative	ADJ
eurjchem-1596	119	3	chromatogram	chromatogram	NOUN
eurjchem-1596	119	4	for	for	ADP
eurjchem-1596	119	5	phosphor‐	phosphor‐	NOUN
eurjchem-1596	119	6	lipid	lipid	NOUN
eurjchem-1596	119	7	elution	elution	NOUN
eurjchem-1596	119	8	and	and	CCONJ
eurjchem-1596	119	9	long	long	ADJ
eurjchem-1596	119	10	runs	run	NOUN
eurjchem-1596	119	11	was	be	AUX
eurjchem-1596	119	12	shown	show	VERB
eurjchem-1596	119	13	in	in	ADP
eurjchem-1596	119	14	figure	figure	NOUN
eurjchem-1596	119	15	2	2	NUM
eurjchem-1596	119	16	.	.	X
eurjchem-1596	119	17	3.2.4	3.2.4	NUM
eurjchem-1596	119	18	.	.	PUNCT
eurjchem-1596	120	1	lower	low	ADJ
eurjchem-1596	120	2	limit	limit	NOUN
eurjchem-1596	120	3	of	of	ADP
eurjchem-1596	120	4	quantification	quantification	NOUN
eurjchem-1596	120	5	or	or	CCONJ
eurjchem-1596	120	6	sensitivity	sensitivity	NOUN
eurjchem-1596	120	7	the	the	DET
eurjchem-1596	120	8	measurable	measurable	ADJ
eurjchem-1596	120	9	lloq	lloq	NOUN
eurjchem-1596	120	10	is	be	AUX
eurjchem-1596	120	11	determined	determine	VERB
eurjchem-1596	120	12	at	at	ADP
eurjchem-1596	120	13	1	1	NUM
eurjchem-1596	120	14	ng	ng	PROPN
eurjchem-1596	120	15	/	/	SYM
eurjchem-1596	120	16	ml	ml	NOUN
eurjchem-1596	120	17	concentration	concentration	NOUN
eurjchem-1596	120	18	.	.	PUNCT
eurjchem-1596	121	1	prepared	prepare	VERB
eurjchem-1596	121	2	and	and	CCONJ
eurjchem-1596	121	3	processed	process	VERB
eurjchem-1596	121	4	6	6	NUM
eurjchem-1596	121	5	replicates	replicate	NOUN
eurjchem-1596	121	6	of	of	ADP
eurjchem-1596	121	7	spiked	spiked	ADJ
eurjchem-1596	121	8	lloq	lloq	NOUN
eurjchem-1596	121	9	plasma	plasma	NOUN
eurjchem-1596	121	10	samples	sample	NOUN
eurjchem-1596	121	11	.	.	PUNCT
eurjchem-1596	122	1	the	the	DET
eurjchem-1596	122	2	average	average	ADJ
eurjchem-1596	122	3	signal	signal	NOUN
eurjchem-1596	122	4	to	to	PART
eurjchem-1596	122	5	noise	noise	NOUN
eurjchem-1596	122	6	ratio	ratio	NOUN
eurjchem-1596	122	7	was	be	AUX
eurjchem-1596	122	8	found	find	VERB
eurjchem-1596	122	9	to	to	PART
eurjchem-1596	122	10	be	be	AUX
eurjchem-1596	122	11	80.1	80.1	NUM
eurjchem-1596	122	12	.	.	PUNCT
eurjchem-1596	123	1	the	the	DET
eurjchem-1596	123	2	precision	precision	NOUN
eurjchem-1596	123	3	(	(	PUNCT
eurjchem-1596	123	4	%	%	INTJ
eurjchem-1596	123	5	rsd	rsd	PROPN
eurjchem-1596	123	6	or	or	CCONJ
eurjchem-1596	123	7	%	%	NOUN
eurjchem-1596	123	8	cv	cv	PROPN
eurjchem-1596	123	9	)	)	PUNCT
eurjchem-1596	123	10	and	and	CCONJ
eurjchem-1596	123	11	accuracy	accuracy	NOUN
eurjchem-1596	123	12	were	be	AUX
eurjchem-1596	123	13	found	find	VERB
eurjchem-1596	123	14	to	to	PART
eurjchem-1596	123	15	be	be	AUX
eurjchem-1596	123	16	7.0	7.0	NUM
eurjchem-1596	123	17	and	and	CCONJ
eurjchem-1596	123	18	94.2	94.2	NUM
eurjchem-1596	123	19	%	%	NOUN
eurjchem-1596	123	20	,	,	PUNCT
eurjchem-1596	123	21	respectively	respectively	ADV
eurjchem-1596	123	22	,	,	PUNCT
eurjchem-1596	123	23	indicates	indicate	VERB
eurjchem-1596	123	24	method	method	NOUN
eurjchem-1596	123	25	reproducibility	reproducibility	NOUN
eurjchem-1596	123	26	at	at	ADP
eurjchem-1596	123	27	lloq	lloq	PROPN
eurjchem-1596	123	28	level	level	NOUN
eurjchem-1596	123	29	.	.	PUNCT
eurjchem-1596	124	1	3.2.5	3.2.5	X
eurjchem-1596	124	2	.	.	X
eurjchem-1596	124	3	method	method	NOUN
eurjchem-1596	124	4	linearity	linearity	NOUN
eurjchem-1596	124	5	linearity	linearity	NOUN
eurjchem-1596	124	6	was	be	AUX
eurjchem-1596	124	7	performed	perform	VERB
eurjchem-1596	124	8	using	use	VERB
eurjchem-1596	124	9	eight	eight	NUM
eurjchem-1596	124	10	calibration	calibration	NOUN
eurjchem-1596	124	11	points	point	NOUN
eurjchem-1596	124	12	(	(	PUNCT
eurjchem-1596	124	13	except	except	SCONJ
eurjchem-1596	124	14	standard	standard	ADJ
eurjchem-1596	124	15	blank	blank	ADJ
eurjchem-1596	124	16	and	and	CCONJ
eurjchem-1596	124	17	standard	standard	ADJ
eurjchem-1596	124	18	zero	zero	NUM
eurjchem-1596	124	19	)	)	PUNCT
eurjchem-1596	124	20	across	across	ADP
eurjchem-1596	124	21	the	the	DET
eurjchem-1596	124	22	calibration	calibration	NOUN
eurjchem-1596	124	23	range	range	NOUN
eurjchem-1596	124	24	of	of	ADP
eurjchem-1596	124	25	1‐300	1‐300	NUM
eurjchem-1596	124	26	ng	ng	PROPN
eurjchem-1596	124	27	/	/	SYM
eurjchem-1596	124	28	ml	ml	PROPN
eurjchem-1596	124	29	(	(	PUNCT
eurjchem-1596	124	30	1	1	NUM
eurjchem-1596	124	31	,	,	PUNCT
eurjchem-1596	124	32	2	2	NUM
eurjchem-1596	124	33	,	,	PUNCT
eurjchem-1596	124	34	5	5	NUM
eurjchem-1596	124	35	,	,	PUNCT
eurjchem-1596	124	36	20	20	NUM
eurjchem-1596	124	37	,	,	PUNCT
eurjchem-1596	124	38	80	80	NUM
eurjchem-1596	124	39	,	,	PUNCT
eurjchem-1596	124	40	160	160	NUM
eurjchem-1596	124	41	,	,	PUNCT
eurjchem-1596	124	42	240	240	NUM
eurjchem-1596	124	43	and	and	CCONJ
eurjchem-1596	124	44	300	300	NUM
eurjchem-1596	124	45	ng	ng	NOUN
eurjchem-1596	124	46	/	/	SYM
eurjchem-1596	124	47	ml	ml	NOUN
eurjchem-1596	124	48	)	)	PUNCT
eurjchem-1596	124	49	.	.	PUNCT
eurjchem-1596	125	1	standard	standard	ADJ
eurjchem-1596	125	2	blank	blank	ADJ
eurjchem-1596	125	3	sample	sample	NOUN
eurjchem-1596	125	4	with	with	ADP
eurjchem-1596	125	5	addition	addition	NOUN
eurjchem-1596	125	6	of	of	ADP
eurjchem-1596	125	7	50	50	NUM
eurjchem-1596	125	8	µl	µl	NOUN
eurjchem-1596	125	9	diluent	diluent	NOUN
eurjchem-1596	125	10	and	and	CCONJ
eurjchem-1596	125	11	standard	standard	ADJ
eurjchem-1596	125	12	zero	zero	NUM
eurjchem-1596	125	13	sample	sample	NOUN
eurjchem-1596	125	14	with	with	ADP
eurjchem-1596	125	15	addition	addition	NOUN
eurjchem-1596	125	16	of	of	ADP
eurjchem-1596	125	17	50	50	NUM
eurjchem-1596	125	18	µl	µl	NOUN
eurjchem-1596	125	19	of	of	ADP
eurjchem-1596	125	20	istd	istd	NOUN
eurjchem-1596	125	21	are	be	AUX
eurjchem-1596	125	22	prepared	prepare	VERB
eurjchem-1596	125	23	along	along	ADP
eurjchem-1596	125	24	with	with	ADP
eurjchem-1596	125	25	calibration	calibration	NOUN
eurjchem-1596	125	26	curve	curve	NOUN
eurjchem-1596	125	27	samples	sample	NOUN
eurjchem-1596	125	28	.	.	PUNCT
eurjchem-1596	126	1	both	both	DET
eurjchem-1596	126	2	samples	sample	NOUN
eurjchem-1596	126	3	were	be	AUX
eurjchem-1596	126	4	used	use	VERB
eurjchem-1596	126	5	to	to	PART
eurjchem-1596	126	6	check	check	VERB
eurjchem-1596	126	7	the	the	DET
eurjchem-1596	126	8	interferences	interference	NOUN
eurjchem-1596	126	9	at	at	ADP
eurjchem-1596	126	10	analyte	analyte	NOUN
eurjchem-1596	126	11	and	and	CCONJ
eurjchem-1596	126	12	istd	istd	PROPN
eurjchem-1596	126	13	retention	retention	PROPN
eurjchem-1596	126	14	times	time	NOUN
eurjchem-1596	126	15	.	.	PUNCT
eurjchem-1596	127	1	the	the	DET
eurjchem-1596	127	2	observed	observe	VERB
eurjchem-1596	127	3	interference	interference	NOUN
eurjchem-1596	127	4	at	at	ADP
eurjchem-1596	127	5	the	the	DET
eurjchem-1596	127	6	retention	retention	NOUN
eurjchem-1596	127	7	time	time	NOUN
eurjchem-1596	127	8	of	of	ADP
eurjchem-1596	127	9	analyte	analyte	NOUN
eurjchem-1596	127	10	and	and	CCONJ
eurjchem-1596	127	11	istd	istd	NOUN
eurjchem-1596	127	12	is	be	AUX
eurjchem-1596	127	13	not	not	PART
eurjchem-1596	127	14	more	more	ADJ
eurjchem-1596	127	15	than	than	ADP
eurjchem-1596	127	16	20	20	NUM
eurjchem-1596	127	17	%	%	NOUN
eurjchem-1596	127	18	and	and	CCONJ
eurjchem-1596	127	19	5	5	NUM
eurjchem-1596	127	20	%	%	NOUN
eurjchem-1596	127	21	,	,	PUNCT
eurjchem-1596	127	22	respectively	respectively	ADV
eurjchem-1596	127	23	.	.	PUNCT
eurjchem-1596	128	1	a	a	DET
eurjchem-1596	128	2	linear	linear	ADJ
eurjchem-1596	128	3	regression	regression	NOUN
eurjchem-1596	128	4	analysis	analysis	NOUN
eurjchem-1596	128	5	with	with	ADP
eurjchem-1596	128	6	weighing	weigh	VERB
eurjchem-1596	128	7	(	(	PUNCT
eurjchem-1596	128	8	1	1	NUM
eurjchem-1596	128	9	/	/	SYM
eurjchem-1596	128	10	x2	x2	NUM
eurjchem-1596	128	11	)	)	PUNCT
eurjchem-1596	128	12	was	be	AUX
eurjchem-1596	128	13	used	use	VERB
eurjchem-1596	128	14	to	to	PART
eurjchem-1596	128	15	determine	determine	VERB
eurjchem-1596	128	16	slopes	slope	NOUN
eurjchem-1596	128	17	,	,	PUNCT
eurjchem-1596	128	18	intercepts	intercept	NOUN
eurjchem-1596	128	19	,	,	PUNCT
eurjchem-1596	128	20	and	and	CCONJ
eurjchem-1596	128	21	correlation	correlation	NOUN
eurjchem-1596	128	22	coefficients	coefficient	NOUN
eurjchem-1596	128	23	.	.	PUNCT
eurjchem-1596	129	1	the	the	DET
eurjchem-1596	129	2	coefficient	coefficient	NOUN
eurjchem-1596	129	3	of	of	ADP
eurjchem-1596	129	4	determination	determination	NOUN
eurjchem-1596	129	5	(	(	PUNCT
eurjchem-1596	129	6	r	r	NOUN
eurjchem-1596	129	7	)	)	PUNCT
eurjchem-1596	129	8	was	be	AUX
eurjchem-1596	129	9	greater	great	ADJ
eurjchem-1596	129	10	than	than	ADP
eurjchem-1596	129	11	0.98	0.98	NUM
eurjchem-1596	129	12	for	for	ADP
eurjchem-1596	129	13	all	all	DET
eurjchem-1596	129	14	the	the	DET
eurjchem-1596	129	15	curves	curve	NOUN
eurjchem-1596	129	16	.	.	PUNCT
eurjchem-1596	130	1	3.2.6	3.2.6	NUM
eurjchem-1596	130	2	.	.	PUNCT
eurjchem-1596	130	3	recovery	recovery	NOUN
eurjchem-1596	130	4	the	the	DET
eurjchem-1596	130	5	extraction	extraction	NOUN
eurjchem-1596	130	6	recovery	recovery	NOUN
eurjchem-1596	130	7	of	of	ADP
eurjchem-1596	130	8	the	the	DET
eurjchem-1596	130	9	analyte	analyte	NOUN
eurjchem-1596	130	10	and	and	CCONJ
eurjchem-1596	130	11	istd	istd	NOUN
eurjchem-1596	130	12	from	from	ADP
eurjchem-1596	130	13	human	human	ADJ
eurjchem-1596	130	14	plasma	plasma	NOUN
eurjchem-1596	130	15	was	be	AUX
eurjchem-1596	130	16	determined	determine	VERB
eurjchem-1596	130	17	by	by	ADP
eurjchem-1596	130	18	comparing	compare	VERB
eurjchem-1596	130	19	each	each	DET
eurjchem-1596	130	20	six	six	NUM
eurjchem-1596	130	21	replicates	replicate	NOUN
eurjchem-1596	130	22	of	of	ADP
eurjchem-1596	130	23	lqc	lqc	PROPN
eurjchem-1596	130	24	,	,	PUNCT
eurjchem-1596	130	25	mqc	mqc	PROPN
eurjchem-1596	130	26	and	and	CCONJ
eurjchem-1596	130	27	hqc	hqc	PROPN
eurjchem-1596	130	28	of	of	ADP
eurjchem-1596	130	29	processed	process	VERB
eurjchem-1596	130	30	samples	sample	NOUN
eurjchem-1596	130	31	with	with	ADP
eurjchem-1596	130	32	that	that	PRON
eurjchem-1596	130	33	of	of	ADP
eurjchem-1596	130	34	respective	respective	ADJ
eurjchem-1596	130	35	post	post	NOUN
eurjchem-1596	130	36	spiked	spiked	ADJ
eurjchem-1596	130	37	samples	sample	NOUN
eurjchem-1596	130	38	.	.	PUNCT
eurjchem-1596	131	1	the	the	DET
eurjchem-1596	131	2	recovery	recovery	NOUN
eurjchem-1596	131	3	at	at	ADP
eurjchem-1596	131	4	lqc	lqc	PROPN
eurjchem-1596	131	5	,	,	PUNCT
eurjchem-1596	131	6	mqc	mqc	PROPN
eurjchem-1596	131	7	and	and	CCONJ
eurjchem-1596	131	8	hqc	hqc	PROPN
eurjchem-1596	131	9	was	be	AUX
eurjchem-1596	131	10	found	find	VERB
eurjchem-1596	131	11	to	to	PART
eurjchem-1596	131	12	be	be	AUX
eurjchem-1596	131	13	61.0	61.0	NUM
eurjchem-1596	131	14	,	,	PUNCT
eurjchem-1596	131	15	65.0	65.0	NUM
eurjchem-1596	131	16	and	and	CCONJ
eurjchem-1596	131	17	63.1	63.1	NUM
eurjchem-1596	131	18	%	%	NOUN
eurjchem-1596	131	19	,	,	PUNCT
eurjchem-1596	131	20	respectively	respectively	ADV
eurjchem-1596	131	21	.	.	PUNCT
eurjchem-1596	132	1	the	the	DET
eurjchem-1596	132	2	overall	overall	ADJ
eurjchem-1596	132	3	average	average	ADJ
eurjchem-1596	132	4	recovery	recovery	NOUN
eurjchem-1596	132	5	of	of	ADP
eurjchem-1596	132	6	analyte	analyte	NOUN
eurjchem-1596	132	7	and	and	CCONJ
eurjchem-1596	132	8	istd	istd	NOUN
eurjchem-1596	132	9	was	be	AUX
eurjchem-1596	132	10	found	find	VERB
eurjchem-1596	132	11	to	to	PART
eurjchem-1596	132	12	be	be	AUX
eurjchem-1596	132	13	63	63	NUM
eurjchem-1596	132	14	and	and	CCONJ
eurjchem-1596	132	15	64.5	64.5	NUM
eurjchem-1596	132	16	%	%	NOUN
eurjchem-1596	132	17	,	,	PUNCT
eurjchem-1596	132	18	respectively	respectively	ADV
eurjchem-1596	132	19	.	.	PUNCT
eurjchem-1596	133	1	use	use	NOUN
eurjchem-1596	133	2	of	of	ADP
eurjchem-1596	133	3	extraction	extraction	NOUN
eurjchem-1596	133	4	solvents	solvent	NOUN
eurjchem-1596	133	5	and	and	CCONJ
eurjchem-1596	133	6	their	their	PRON
eurjchem-1596	133	7	combinations	combination	NOUN
eurjchem-1596	133	8	(	(	PUNCT
eurjchem-1596	133	9	section	section	NOUN
eurjchem-1596	133	10	3.1.3	3.1.3	NUM
eurjchem-1596	133	11	)	)	PUNCT
eurjchem-1596	133	12	results	result	NOUN
eurjchem-1596	133	13	in	in	ADP
eurjchem-1596	133	14	variable	variable	ADJ
eurjchem-1596	133	15	recoveries	recovery	NOUN
eurjchem-1596	133	16	for	for	ADP
eurjchem-1596	133	17	analyte	analyte	NOUN
eurjchem-1596	133	18	and	and	CCONJ
eurjchem-1596	133	19	istd	istd	NOUN
eurjchem-1596	133	20	,	,	PUNCT
eurjchem-1596	133	21	but	but	CCONJ
eurjchem-1596	133	22	finally	finally	ADV
eurjchem-1596	133	23	similar	similar	ADJ
eurjchem-1596	133	24	recovery	recovery	NOUN
eurjchem-1596	133	25	for	for	ADP
eurjchem-1596	133	26	both	both	DET
eurjchem-1596	133	27	analyte	analyte	NOUN
eurjchem-1596	133	28	and	and	CCONJ
eurjchem-1596	133	29	istd	istd	NOUN
eurjchem-1596	133	30	were	be	AUX
eurjchem-1596	133	31	achieved	achieve	VERB
eurjchem-1596	133	32	with	with	ADP
eurjchem-1596	133	33	proposed	propose	VERB
eurjchem-1596	133	34	extraction	extraction	NOUN
eurjchem-1596	133	35	solvent	solvent	NOUN
eurjchem-1596	133	36	which	which	PRON
eurjchem-1596	133	37	nullifies	nullify	VERB
eurjchem-1596	133	38	the	the	DET
eurjchem-1596	133	39	matrix	matrix	NOUN
eurjchem-1596	133	40	effect	effect	NOUN
eurjchem-1596	133	41	.	.	PUNCT
eurjchem-1596	134	1	the	the	DET
eurjchem-1596	134	2	mean	mean	ADJ
eurjchem-1596	134	3	observed	observe	VERB
eurjchem-1596	134	4	recoveries	recovery	NOUN
eurjchem-1596	134	5	of	of	ADP
eurjchem-1596	134	6	both	both	DET
eurjchem-1596	134	7	analyte	analyte	NOUN
eurjchem-1596	134	8	and	and	CCONJ
eurjchem-1596	134	9	istd	istd	NOUN
eurjchem-1596	134	10	were	be	AUX
eurjchem-1596	134	11	shown	show	VERB
eurjchem-1596	134	12	in	in	ADP
eurjchem-1596	134	13	table	table	NOUN
eurjchem-1596	134	14	2	2	NUM
eurjchem-1596	134	15	.	.	X
eurjchem-1596	134	16	262	262	NUM
eurjchem-1596	134	17	pappula	pappula	NOUN
eurjchem-1596	134	18	et	et	PROPN
eurjchem-1596	134	19	al	al	PROPN
eurjchem-1596	134	20	.	.	PUNCT
eurjchem-1596	134	21	/	/	SYM
eurjchem-1596	134	22	european	european	PROPN
eurjchem-1596	134	23	journal	journal	PROPN
eurjchem-1596	134	24	of	of	ADP
eurjchem-1596	134	25	chemistry	chemistry	NOUN
eurjchem-1596	134	26	8	8	NUM
eurjchem-1596	134	27	(	(	PUNCT
eurjchem-1596	134	28	3	3	NUM
eurjchem-1596	134	29	)	)	PUNCT
eurjchem-1596	134	30	(	(	PUNCT
eurjchem-1596	134	31	2017	2017	NUM
eurjchem-1596	134	32	)	)	PUNCT
eurjchem-1596	134	33	258‐264	258‐264	NUM
eurjchem-1596	134	34	table	table	NOUN
eurjchem-1596	134	35	3	3	NUM
eurjchem-1596	134	36	.	.	NOUN
eurjchem-1596	134	37	precision	precision	NOUN
eurjchem-1596	134	38	and	and	CCONJ
eurjchem-1596	134	39	accuracy	accuracy	NOUN
eurjchem-1596	134	40	of	of	ADP
eurjchem-1596	134	41	ulipristal	ulipristal	ADJ
eurjchem-1596	134	42	acetate	acetate	NOUN
eurjchem-1596	134	43	in	in	ADP
eurjchem-1596	134	44	human	human	ADJ
eurjchem-1596	134	45	plasma	plasma	NOUN
eurjchem-1596	134	46	samples	sample	NOUN
eurjchem-1596	134	47	.	.	PUNCT
eurjchem-1596	135	1	sample	sample	NOUN
eurjchem-1596	135	2	name	name	NOUN
eurjchem-1596	135	3	conc	conc	NOUN
eurjchem-1596	135	4	.	.	PUNCT
eurjchem-1596	136	1	added	add	VERB
eurjchem-1596	136	2	(	(	PUNCT
eurjchem-1596	136	3	ng	ng	PROPN
eurjchem-1596	136	4	/	/	SYM
eurjchem-1596	136	5	ml	ml	NOUN
eurjchem-1596	136	6	)	)	PUNCT
eurjchem-1596	136	7	within	within	ADP
eurjchem-1596	136	8	batch	batch	NOUN
eurjchem-1596	136	9	(	(	PUNCT
eurjchem-1596	136	10	n=12	n=12	NOUN
eurjchem-1596	136	11	)	)	PUNCT
eurjchem-1596	136	12	between	between	ADP
eurjchem-1596	136	13	batch	batch	NOUN
eurjchem-1596	136	14	(	(	PUNCT
eurjchem-1596	136	15	n=18	n=18	ADJ
eurjchem-1596	136	16	)	)	PUNCT
eurjchem-1596	136	17	conc	conc	NOUN
eurjchem-1596	136	18	.	.	PUNCT
eurjchem-1596	137	1	found	find	VERB
eurjchem-1596	137	2	(	(	PUNCT
eurjchem-1596	137	3	ng	ng	NOUN
eurjchem-1596	137	4	/	/	SYM
eurjchem-1596	137	5	ml	ml	NOUN
eurjchem-1596	137	6	)	)	PUNCT
eurjchem-1596	137	7	mean±sd	mean±sd	ADP
eurjchem-1596	137	8	precision	precision	NOUN
eurjchem-1596	137	9	(	(	PUNCT
eurjchem-1596	137	10	%	%	INTJ
eurjchem-1596	137	11	)	)	PUNCT
eurjchem-1596	137	12	accuracy	accuracy	NOUN
eurjchem-1596	137	13	(	(	PUNCT
eurjchem-1596	137	14	%	%	INTJ
eurjchem-1596	137	15	)	)	PUNCT
eurjchem-1596	137	16	conc	conc	NOUN
eurjchem-1596	137	17	.	.	PUNCT
eurjchem-1596	138	1	found	find	VERB
eurjchem-1596	138	2	(	(	PUNCT
eurjchem-1596	138	3	ng	ng	NOUN
eurjchem-1596	138	4	/	/	SYM
eurjchem-1596	138	5	ml	ml	NOUN
eurjchem-1596	138	6	)	)	PUNCT
eurjchem-1596	138	7	mean±sd	mean±sd	ADP
eurjchem-1596	138	8	precision	precision	NOUN
eurjchem-1596	138	9	(	(	PUNCT
eurjchem-1596	138	10	%	%	INTJ
eurjchem-1596	138	11	)	)	PUNCT
eurjchem-1596	138	12	accuracy	accuracy	NOUN
eurjchem-1596	138	13	(	(	PUNCT
eurjchem-1596	138	14	%	%	INTJ
eurjchem-1596	138	15	)	)	PUNCT
eurjchem-1596	138	16	lloqqc	lloqqc	NOUN
eurjchem-1596	138	17	1	1	NUM
eurjchem-1596	138	18	0.9±0.1	0.9±0.1	NOUN
eurjchem-1596	138	19	7.0	7.0	NUM
eurjchem-1596	138	20	94.2	94.2	NUM
eurjchem-1596	138	21	1.0±0.1	1.0±0.1	NUM
eurjchem-1596	138	22	6.3	6.3	NUM
eurjchem-1596	138	23	95.6	95.6	NUM
eurjchem-1596	138	24	lqc	lqc	NOUN
eurjchem-1596	138	25	3	3	NUM
eurjchem-1596	138	26	3.0±0.1	3.0±0.1	NUM
eurjchem-1596	138	27	3.9	3.9	NUM
eurjchem-1596	138	28	98.6	98.6	NUM
eurjchem-1596	138	29	3.0±0.1	3.0±0.1	NUM
eurjchem-1596	138	30	4.0	4.0	NUM
eurjchem-1596	138	31	98.3	98.3	NUM
eurjchem-1596	138	32	mqc	mqc	NOUN
eurjchem-1596	138	33	126	126	NUM
eurjchem-1596	138	34	127.7±3.5	127.7±3.5	NUM
eurjchem-1596	138	35	2.7	2.7	NUM
eurjchem-1596	138	36	98.7	98.7	NUM
eurjchem-1596	138	37	126.4±5.5	126.4±5.5	NUM
eurjchem-1596	138	38	4.4	4.4	NUM
eurjchem-1596	138	39	99.7	99.7	NUM
eurjchem-1596	138	40	hqc	hqc	PROPN
eurjchem-1596	138	41	228	228	NUM
eurjchem-1596	138	42	232.6±8.7	232.6±8.7	NUM
eurjchem-1596	138	43	3.7	3.7	NUM
eurjchem-1596	138	44	98.0	98.0	NUM
eurjchem-1596	138	45	232.4±7.3	232.4±7.3	NUM
eurjchem-1596	138	46	3.1	3.1	NUM
eurjchem-1596	138	47	98.1	98.1	NUM
eurjchem-1596	138	48	dqc	dqc	NOUN
eurjchem-1596	138	49	600	600	NUM
eurjchem-1596	138	50	610.9±12.5	610.9±12.5	NOUN
eurjchem-1596	138	51	2.1	2.1	NUM
eurjchem-1596	138	52	98.2	98.2	NUM
eurjchem-1596	138	53	607.9±14.0	607.9±14.0	NUM
eurjchem-1596	138	54	2.3	2.3	NUM
eurjchem-1596	138	55	98.7	98.7	NUM
eurjchem-1596	138	56	the	the	DET
eurjchem-1596	138	57	very	very	ADV
eurjchem-1596	138	58	near	near	ADJ
eurjchem-1596	138	59	recovery	recovery	NOUN
eurjchem-1596	138	60	of	of	ADP
eurjchem-1596	138	61	analyte	analyte	NOUN
eurjchem-1596	138	62	and	and	CCONJ
eurjchem-1596	138	63	istd	istd	NOUN
eurjchem-1596	138	64	in	in	ADP
eurjchem-1596	138	65	turn	turn	NOUN
eurjchem-1596	138	66	indicates	indicate	VERB
eurjchem-1596	138	67	similar	similar	ADJ
eurjchem-1596	138	68	behaviour	behaviour	NOUN
eurjchem-1596	138	69	of	of	ADP
eurjchem-1596	138	70	analyte	analyte	NOUN
eurjchem-1596	138	71	and	and	CCONJ
eurjchem-1596	138	72	istd	istd	NOUN
eurjchem-1596	138	73	.	.	PUNCT
eurjchem-1596	139	1	the	the	DET
eurjchem-1596	139	2	intensity	intensity	NOUN
eurjchem-1596	139	3	of	of	ADP
eurjchem-1596	139	4	analyte	analyte	NOUN
eurjchem-1596	139	5	and	and	CCONJ
eurjchem-1596	139	6	istd	istd	NOUN
eurjchem-1596	139	7	in	in	ADP
eurjchem-1596	139	8	presence	presence	NOUN
eurjchem-1596	139	9	and	and	CCONJ
eurjchem-1596	139	10	absence	absence	NOUN
eurjchem-1596	139	11	of	of	ADP
eurjchem-1596	139	12	biological	biological	ADJ
eurjchem-1596	139	13	matrix	matrix	NOUN
eurjchem-1596	139	14	indicates	indicate	VERB
eurjchem-1596	139	15	congener	congener	NOUN
eurjchem-1596	139	16	behaviour	behaviour	PROPN
eurjchem-1596	139	17	and	and	CCONJ
eurjchem-1596	139	18	levonorgestrel	levonorgestrel	NOUN
eurjchem-1596	139	19	suitability	suitability	NOUN
eurjchem-1596	139	20	as	as	ADP
eurjchem-1596	139	21	istd	istd	NOUN
eurjchem-1596	139	22	.	.	PUNCT
eurjchem-1596	140	1	so	so	ADV
eurjchem-1596	140	2	,	,	PUNCT
eurjchem-1596	140	3	the	the	DET
eurjchem-1596	140	4	method	method	NOUN
eurjchem-1596	140	5	mimics	mimic	VERB
eurjchem-1596	140	6	the	the	DET
eurjchem-1596	140	7	characteristics	characteristic	NOUN
eurjchem-1596	140	8	of	of	ADP
eurjchem-1596	140	9	isotope	isotope	NOUN
eurjchem-1596	140	10	labelled	label	VERB
eurjchem-1596	140	11	internal	internal	ADJ
eurjchem-1596	140	12	standard	standard	NOUN
eurjchem-1596	140	13	.	.	PUNCT
eurjchem-1596	141	1	based	base	VERB
eurjchem-1596	141	2	on	on	ADP
eurjchem-1596	141	3	this	this	PRON
eurjchem-1596	141	4	,	,	PUNCT
eurjchem-1596	141	5	we	we	PRON
eurjchem-1596	141	6	conclude	conclude	VERB
eurjchem-1596	141	7	levonorgestrel	levonorgestrel	NOUN
eurjchem-1596	141	8	is	be	AUX
eurjchem-1596	141	9	suitable	suitable	ADJ
eurjchem-1596	141	10	internal	internal	ADJ
eurjchem-1596	141	11	standard	standard	NOUN
eurjchem-1596	141	12	for	for	ADP
eurjchem-1596	141	13	quantification	quantification	NOUN
eurjchem-1596	141	14	of	of	ADP
eurjchem-1596	141	15	ulipristal	ulipristal	ADJ
eurjchem-1596	141	16	acetate	acetate	NOUN
eurjchem-1596	141	17	.	.	PUNCT
eurjchem-1596	142	1	3.2.7	3.2.7	NUM
eurjchem-1596	142	2	.	.	PUNCT
eurjchem-1596	142	3	precision	precision	NOUN
eurjchem-1596	142	4	and	and	CCONJ
eurjchem-1596	142	5	accuracy	accuracy	NOUN
eurjchem-1596	142	6	it	it	PRON
eurjchem-1596	142	7	is	be	AUX
eurjchem-1596	142	8	evaluated	evaluate	VERB
eurjchem-1596	142	9	by	by	ADP
eurjchem-1596	142	10	performing	perform	VERB
eurjchem-1596	142	11	three	three	NUM
eurjchem-1596	142	12	different	different	ADJ
eurjchem-1596	142	13	batches	batch	NOUN
eurjchem-1596	142	14	on	on	ADP
eurjchem-1596	142	15	two	two	NUM
eurjchem-1596	142	16	days	day	NOUN
eurjchem-1596	142	17	,	,	PUNCT
eurjchem-1596	142	18	each	each	PRON
eurjchem-1596	142	19	consists	consist	VERB
eurjchem-1596	142	20	of	of	ADP
eurjchem-1596	142	21	six	six	NUM
eurjchem-1596	142	22	replicates	replicate	NOUN
eurjchem-1596	142	23	of	of	ADP
eurjchem-1596	142	24	five	five	NUM
eurjchem-1596	142	25	qc	qc	PROPN
eurjchem-1596	142	26	concent‐	concent‐	PROPN
eurjchem-1596	142	27	ration	ration	NOUN
eurjchem-1596	142	28	levels	level	NOUN
eurjchem-1596	142	29	(	(	PUNCT
eurjchem-1596	142	30	lloqqc	lloqqc	NOUN
eurjchem-1596	142	31	,	,	PUNCT
eurjchem-1596	142	32	lqc	lqc	PROPN
eurjchem-1596	142	33	,	,	PUNCT
eurjchem-1596	142	34	mqc	mqc	PROPN
eurjchem-1596	142	35	,	,	PUNCT
eurjchem-1596	142	36	hqc	hqc	INTJ
eurjchem-1596	142	37	,	,	PUNCT
eurjchem-1596	142	38	and	and	CCONJ
eurjchem-1596	142	39	dqc	dqc	VERB
eurjchem-1596	142	40	ng	ng	PROPN
eurjchem-1596	142	41	/	/	SYM
eurjchem-1596	142	42	ml	ml	NOUN
eurjchem-1596	142	43	)	)	PUNCT
eurjchem-1596	142	44	over	over	ADP
eurjchem-1596	142	45	calibration	calibration	NOUN
eurjchem-1596	142	46	range	range	NOUN
eurjchem-1596	142	47	to	to	PART
eurjchem-1596	142	48	ensure	ensure	VERB
eurjchem-1596	142	49	inter	inter	ADJ
eurjchem-1596	142	50	(	(	PUNCT
eurjchem-1596	142	51	different	different	ADJ
eurjchem-1596	142	52	days	day	NOUN
eurjchem-1596	142	53	)	)	PUNCT
eurjchem-1596	142	54	and	and	CCONJ
eurjchem-1596	142	55	intraday	intraday	NOUN
eurjchem-1596	142	56	(	(	PUNCT
eurjchem-1596	142	57	within	within	ADP
eurjchem-1596	142	58	day	day	NOUN
eurjchem-1596	142	59	)	)	PUNCT
eurjchem-1596	142	60	precision	precision	NOUN
eurjchem-1596	142	61	and	and	CCONJ
eurjchem-1596	142	62	accuracy	accuracy	NOUN
eurjchem-1596	142	63	.	.	PUNCT
eurjchem-1596	143	1	the	the	DET
eurjchem-1596	143	2	mean	mean	ADJ
eurjchem-1596	143	3	back	back	ADP
eurjchem-1596	143	4	calculated	calculate	VERB
eurjchem-1596	143	5	concentrations	concentration	NOUN
eurjchem-1596	143	6	(	(	PUNCT
eurjchem-1596	143	7	accuracy	accuracy	NOUN
eurjchem-1596	143	8	)	)	PUNCT
eurjchem-1596	143	9	and	and	CCONJ
eurjchem-1596	143	10	their	their	PRON
eurjchem-1596	143	11	reproducibility	reproducibility	NOUN
eurjchem-1596	143	12	(	(	PUNCT
eurjchem-1596	143	13	preci‐	preci‐	NOUN
eurjchem-1596	143	14	sion	sion	PROPN
eurjchem-1596	143	15	)	)	PUNCT
eurjchem-1596	143	16	at	at	ADP
eurjchem-1596	143	17	each	each	DET
eurjchem-1596	143	18	concentration	concentration	NOUN
eurjchem-1596	143	19	level	level	NOUN
eurjchem-1596	143	20	were	be	AUX
eurjchem-1596	143	21	shown	show	VERB
eurjchem-1596	143	22	in	in	ADP
eurjchem-1596	143	23	table	table	NOUN
eurjchem-1596	143	24	3	3	NUM
eurjchem-1596	143	25	.	.	PUNCT
eurjchem-1596	144	1	the	the	DET
eurjchem-1596	144	2	intraday	intraday	NOUN
eurjchem-1596	144	3	(	(	PUNCT
eurjchem-1596	144	4	average	average	NOUN
eurjchem-1596	144	5	of	of	ADP
eurjchem-1596	144	6	12	12	NUM
eurjchem-1596	144	7	replicates	replicate	NOUN
eurjchem-1596	144	8	)	)	PUNCT
eurjchem-1596	144	9	and	and	CCONJ
eurjchem-1596	144	10	inter‐day	inter‐day	PROPN
eurjchem-1596	144	11	(	(	PUNCT
eurjchem-1596	144	12	average	average	NOUN
eurjchem-1596	144	13	of	of	ADP
eurjchem-1596	144	14	18	18	NUM
eurjchem-1596	144	15	replicates	replicate	NOUN
eurjchem-1596	144	16	)	)	PUNCT
eurjchem-1596	144	17	precision	precision	NOUN
eurjchem-1596	144	18	(	(	PUNCT
eurjchem-1596	144	19	%	%	INTJ
eurjchem-1596	144	20	cv	cv	PROPN
eurjchem-1596	144	21	)	)	PUNCT
eurjchem-1596	144	22	was	be	AUX
eurjchem-1596	144	23	less	less	ADJ
eurjchem-1596	144	24	than	than	ADP
eurjchem-1596	144	25	7.0	7.0	NUM
eurjchem-1596	144	26	%	%	NOUN
eurjchem-1596	144	27	and	and	CCONJ
eurjchem-1596	144	28	the	the	DET
eurjchem-1596	144	29	accuracy	accuracy	NOUN
eurjchem-1596	144	30	was	be	AUX
eurjchem-1596	144	31	in	in	ADP
eurjchem-1596	144	32	the	the	DET
eurjchem-1596	144	33	range	range	NOUN
eurjchem-1596	144	34	of	of	ADP
eurjchem-1596	144	35	94.2	94.2	NUM
eurjchem-1596	144	36	to	to	PART
eurjchem-1596	144	37	99.7	99.7	NUM
eurjchem-1596	144	38	%	%	NOUN
eurjchem-1596	144	39	.	.	PUNCT
eurjchem-1596	145	1	the	the	DET
eurjchem-1596	145	2	obtained	obtain	VERB
eurjchem-1596	145	3	result	result	NOUN
eurjchem-1596	145	4	proves	prove	VERB
eurjchem-1596	145	5	that	that	SCONJ
eurjchem-1596	145	6	the	the	DET
eurjchem-1596	145	7	method	method	NOUN
eurjchem-1596	145	8	was	be	AUX
eurjchem-1596	145	9	rugged	rugged	ADJ
eurjchem-1596	145	10	and	and	CCONJ
eurjchem-1596	145	11	reproducible	reproducible	ADJ
eurjchem-1596	145	12	over	over	ADP
eurjchem-1596	145	13	the	the	DET
eurjchem-1596	145	14	proposed	propose	VERB
eurjchem-1596	145	15	analytical	analytical	ADJ
eurjchem-1596	145	16	range	range	NOUN
eurjchem-1596	145	17	.	.	PUNCT
eurjchem-1596	146	1	the	the	DET
eurjchem-1596	146	2	repre‐	repre‐	NOUN
eurjchem-1596	146	3	sentative	sentative	ADJ
eurjchem-1596	146	4	chromatograms	chromatogram	NOUN
eurjchem-1596	146	5	of	of	ADP
eurjchem-1596	146	6	blank	blank	ADJ
eurjchem-1596	146	7	plasma	plasma	NOUN
eurjchem-1596	146	8	,	,	PUNCT
eurjchem-1596	146	9	lower	low	ADJ
eurjchem-1596	146	10	limit	limit	NOUN
eurjchem-1596	146	11	of	of	ADP
eurjchem-1596	146	12	quantification	quantification	NOUN
eurjchem-1596	146	13	(	(	PUNCT
eurjchem-1596	146	14	lloq	lloq	NOUN
eurjchem-1596	146	15	)	)	PUNCT
eurjchem-1596	146	16	and	and	CCONJ
eurjchem-1596	146	17	upper	upper	ADJ
eurjchem-1596	146	18	limit	limit	NOUN
eurjchem-1596	146	19	of	of	ADP
eurjchem-1596	146	20	quantification	quantification	NOUN
eurjchem-1596	146	21	(	(	PUNCT
eurjchem-1596	146	22	uloq	uloq	NOUN
eurjchem-1596	146	23	)	)	PUNCT
eurjchem-1596	146	24	level	level	NOUN
eurjchem-1596	146	25	for	for	ADP
eurjchem-1596	146	26	analyte	analyte	NOUN
eurjchem-1596	146	27	and	and	CCONJ
eurjchem-1596	146	28	istd	istd	NOUN
eurjchem-1596	146	29	were	be	AUX
eurjchem-1596	146	30	shown	show	VERB
eurjchem-1596	146	31	in	in	ADP
eurjchem-1596	146	32	figure	figure	NOUN
eurjchem-1596	146	33	3	3	NUM
eurjchem-1596	146	34	to	to	ADP
eurjchem-1596	146	35	5	5	NUM
eurjchem-1596	146	36	,	,	PUNCT
eurjchem-1596	146	37	respectively	respectively	ADV
eurjchem-1596	146	38	.	.	PUNCT
eurjchem-1596	147	1	(	(	PUNCT
eurjchem-1596	147	2	a	a	X
eurjchem-1596	147	3	)	)	PUNCT
eurjchem-1596	147	4	(	(	PUNCT
eurjchem-1596	147	5	b	b	X
eurjchem-1596	147	6	)	)	PUNCT
eurjchem-1596	147	7	figure	figure	NOUN
eurjchem-1596	147	8	3	3	NUM
eurjchem-1596	147	9	.	.	PUNCT
eurjchem-1596	148	1	blank	blank	ADJ
eurjchem-1596	148	2	plasma	plasma	NOUN
eurjchem-1596	148	3	chromatogram	chromatogram	PROPN
eurjchem-1596	148	4	of	of	ADP
eurjchem-1596	148	5	(	(	PUNCT
eurjchem-1596	148	6	a	a	PRON
eurjchem-1596	148	7	)	)	PUNCT
eurjchem-1596	148	8	ulipristal	ulipristal	ADJ
eurjchem-1596	148	9	acetate	acetate	NOUN
eurjchem-1596	148	10	and	and	CCONJ
eurjchem-1596	148	11	(	(	PUNCT
eurjchem-1596	148	12	b	b	NOUN
eurjchem-1596	148	13	)	)	PUNCT
eurjchem-1596	148	14	levonorgestrel	levonorgestrel	NOUN
eurjchem-1596	148	15	.	.	PUNCT
eurjchem-1596	149	1	(	(	PUNCT
eurjchem-1596	149	2	a	a	X
eurjchem-1596	149	3	)	)	PUNCT
eurjchem-1596	149	4	(	(	PUNCT
eurjchem-1596	149	5	b	b	X
eurjchem-1596	149	6	)	)	PUNCT
eurjchem-1596	149	7	figure	figure	NOUN
eurjchem-1596	149	8	4	4	NUM
eurjchem-1596	149	9	.	.	NOUN
eurjchem-1596	149	10	chromatograms	chromatogram	NOUN
eurjchem-1596	149	11	of	of	ADP
eurjchem-1596	149	12	(	(	PUNCT
eurjchem-1596	149	13	a	a	PRON
eurjchem-1596	149	14	)	)	PUNCT
eurjchem-1596	149	15	ulipristal	ulipristal	ADJ
eurjchem-1596	149	16	acetate	acetate	NOUN
eurjchem-1596	149	17	and	and	CCONJ
eurjchem-1596	149	18	(	(	PUNCT
eurjchem-1596	149	19	b	b	NOUN
eurjchem-1596	149	20	)	)	PUNCT
eurjchem-1596	149	21	levonorgestrel	levonorgestrel	NOUN
eurjchem-1596	149	22	at	at	ADP
eurjchem-1596	149	23	lloq	lloq	PROPN
eurjchem-1596	149	24	level	level	NOUN
eurjchem-1596	149	25	.	.	PUNCT
eurjchem-1596	150	1	3.2.8	3.2.8	X
eurjchem-1596	150	2	.	.	PUNCT
eurjchem-1596	150	3	dilution	dilution	NOUN
eurjchem-1596	150	4	integrity	integrity	NOUN
eurjchem-1596	150	5	(	(	PUNCT
eurjchem-1596	150	6	dqc	dqc	PROPN
eurjchem-1596	150	7	)	)	PUNCT
eurjchem-1596	150	8	the	the	DET
eurjchem-1596	150	9	interference	interference	NOUN
eurjchem-1596	150	10	free	free	ADJ
eurjchem-1596	150	11	(	(	PUNCT
eurjchem-1596	150	12	screened	screen	VERB
eurjchem-1596	150	13	)	)	PUNCT
eurjchem-1596	150	14	plasma	plasma	NOUN
eurjchem-1596	150	15	lot	lot	NOUN
eurjchem-1596	150	16	was	be	AUX
eurjchem-1596	150	17	spiked	spike	VERB
eurjchem-1596	150	18	to	to	PART
eurjchem-1596	150	19	get	get	VERB
eurjchem-1596	150	20	the	the	DET
eurjchem-1596	150	21	concentration	concentration	NOUN
eurjchem-1596	150	22	approximately	approximately	ADV
eurjchem-1596	150	23	double	double	DET
eurjchem-1596	150	24	the	the	DET
eurjchem-1596	150	25	uloq	uloq	NOUN
eurjchem-1596	150	26	,	,	PUNCT
eurjchem-1596	150	27	i.e	i.e	PROPN
eurjchem-1596	150	28	600	600	NUM
eurjchem-1596	150	29	ng	ng	NOUN
eurjchem-1596	150	30	/	/	SYM
eurjchem-1596	150	31	ml	ml	NOUN
eurjchem-1596	150	32	of	of	ADP
eurjchem-1596	150	33	analyte	analyte	NOUN
eurjchem-1596	150	34	and	and	CCONJ
eurjchem-1596	150	35	the	the	DET
eurjchem-1596	150	36	sample	sample	NOUN
eurjchem-1596	150	37	was	be	AUX
eurjchem-1596	150	38	further	far	ADV
eurjchem-1596	150	39	diluted	dilute	VERB
eurjchem-1596	150	40	(	(	PUNCT
eurjchem-1596	150	41	1/4	1/4	NUM
eurjchem-1596	150	42	)	)	PUNCT
eurjchem-1596	150	43	to	to	PART
eurjchem-1596	150	44	get	get	VERB
eurjchem-1596	150	45	dqc	dqc	ADJ
eurjchem-1596	150	46	sample	sample	NOUN
eurjchem-1596	150	47	.	.	PUNCT
eurjchem-1596	151	1	the	the	DET
eurjchem-1596	151	2	precision	precision	NOUN
eurjchem-1596	151	3	and	and	CCONJ
eurjchem-1596	151	4	accuracy	accuracy	NOUN
eurjchem-1596	151	5	(	(	PUNCT
eurjchem-1596	151	6	n=6	n=6	NOUN
eurjchem-1596	151	7	)	)	PUNCT
eurjchem-1596	151	8	was	be	AUX
eurjchem-1596	151	9	found	find	VERB
eurjchem-1596	151	10	to	to	PART
eurjchem-1596	151	11	be	be	AUX
eurjchem-1596	151	12	2.0	2.0	NUM
eurjchem-1596	151	13	and	and	CCONJ
eurjchem-1596	151	14	98.1	98.1	NUM
eurjchem-1596	151	15	%	%	NOUN
eurjchem-1596	151	16	,	,	PUNCT
eurjchem-1596	151	17	respectively	respectively	ADV
eurjchem-1596	151	18	.	.	PUNCT
eurjchem-1596	152	1	3.2.9	3.2.9	X
eurjchem-1596	152	2	.	.	PUNCT
eurjchem-1596	152	3	stability	stability	NOUN
eurjchem-1596	152	4	in	in	ADP
eurjchem-1596	152	5	plasma	plasma	NOUN
eurjchem-1596	152	6	and	and	CCONJ
eurjchem-1596	152	7	processed	process	VERB
eurjchem-1596	152	8	samples	sample	NOUN
eurjchem-1596	152	9	stability	stability	NOUN
eurjchem-1596	152	10	of	of	ADP
eurjchem-1596	152	11	the	the	DET
eurjchem-1596	152	12	ulipristal	ulipristal	ADJ
eurjchem-1596	152	13	acetate	acetate	NOUN
eurjchem-1596	152	14	in	in	ADP
eurjchem-1596	152	15	human	human	ADJ
eurjchem-1596	152	16	plasma	plasma	NOUN
eurjchem-1596	152	17	(	(	PUNCT
eurjchem-1596	152	18	bench	bench	VERB
eurjchem-1596	152	19	top	top	ADJ
eurjchem-1596	152	20	stability	stability	NOUN
eurjchem-1596	152	21	,	,	PUNCT
eurjchem-1596	152	22	freeze	freeze	VERB
eurjchem-1596	152	23	and	and	CCONJ
eurjchem-1596	152	24	thaw	thaw	NOUN
eurjchem-1596	152	25	stability	stability	NOUN
eurjchem-1596	152	26	,	,	PUNCT
eurjchem-1596	152	27	long	long	ADJ
eurjchem-1596	152	28	term	term	NOUN
eurjchem-1596	152	29	stability	stability	NOUN
eurjchem-1596	152	30	in	in	ADP
eurjchem-1596	152	31	matrix	matrix	NOUN
eurjchem-1596	152	32	)	)	PUNCT
eurjchem-1596	152	33	and	and	CCONJ
eurjchem-1596	152	34	in	in	ADP
eurjchem-1596	152	35	the	the	DET
eurjchem-1596	152	36	processed	process	VERB
eurjchem-1596	152	37	samples	sample	NOUN
eurjchem-1596	152	38	(	(	PUNCT
eurjchem-1596	152	39	dry	dry	ADJ
eurjchem-1596	152	40	extract	extract	NOUN
eurjchem-1596	152	41	stability	stability	NOUN
eurjchem-1596	152	42	,	,	PUNCT
eurjchem-1596	152	43	in‐	in‐	SCONJ
eurjchem-1596	152	44	injector	injector	NOUN
eurjchem-1596	152	45	stability	stability	NOUN
eurjchem-1596	152	46	and	and	CCONJ
eurjchem-1596	152	47	re‐injection	re‐injection	NOUN
eurjchem-1596	152	48	reproducibility	reproducibility	NOUN
eurjchem-1596	152	49	)	)	PUNCT
eurjchem-1596	152	50	were	be	AUX
eurjchem-1596	152	51	assessed	assess	VERB
eurjchem-1596	152	52	as	as	ADP
eurjchem-1596	152	53	a	a	DET
eurjchem-1596	152	54	part	part	NOUN
eurjchem-1596	152	55	of	of	ADP
eurjchem-1596	152	56	method	method	NOUN
eurjchem-1596	152	57	validation	validation	NOUN
eurjchem-1596	152	58	.	.	PUNCT
eurjchem-1596	153	1	for	for	ADP
eurjchem-1596	153	2	all	all	DET
eurjchem-1596	153	3	stability	stability	NOUN
eurjchem-1596	153	4	experi‐	experi‐	X
eurjchem-1596	153	5	ments	ment	NOUN
eurjchem-1596	153	6	,	,	PUNCT
eurjchem-1596	153	7	six	six	NUM
eurjchem-1596	153	8	replicates	replicate	NOUN
eurjchem-1596	153	9	of	of	ADP
eurjchem-1596	153	10	lqc	lqc	NOUN
eurjchem-1596	153	11	and	and	CCONJ
eurjchem-1596	153	12	hqc	hqc	ADP
eurjchem-1596	153	13	stability	stability	NOUN
eurjchem-1596	153	14	samples	sample	NOUN
eurjchem-1596	153	15	were	be	AUX
eurjchem-1596	153	16	processed	process	VERB
eurjchem-1596	153	17	and	and	CCONJ
eurjchem-1596	153	18	evaluated	evaluate	VERB
eurjchem-1596	153	19	against	against	ADP
eurjchem-1596	153	20	freshly	freshly	ADV
eurjchem-1596	153	21	prepared	prepare	VERB
eurjchem-1596	153	22	calibration	calibration	NOUN
eurjchem-1596	153	23	curve	curve	NOUN
eurjchem-1596	153	24	.	.	PUNCT
eurjchem-1596	154	1	in	in	SCONJ
eurjchem-1596	154	2	case	case	NOUN
eurjchem-1596	154	3	of	of	ADP
eurjchem-1596	154	4	long	long	ADJ
eurjchem-1596	154	5	term	term	NOUN
eurjchem-1596	154	6	stability	stability	NOUN
eurjchem-1596	154	7	experiments	experiment	VERB
eurjchem-1596	154	8	fresh	fresh	ADJ
eurjchem-1596	154	9	stock	stock	NOUN
eurjchem-1596	154	10	weighing	weighing	NOUN
eurjchem-1596	154	11	was	be	AUX
eurjchem-1596	154	12	done	do	VERB
eurjchem-1596	154	13	on	on	ADP
eurjchem-1596	154	14	the	the	DET
eurjchem-1596	154	15	day	day	NOUN
eurjchem-1596	154	16	of	of	ADP
eurjchem-1596	154	17	evaluation	evaluation	NOUN
eurjchem-1596	154	18	.	.	PUNCT
eurjchem-1596	155	1	samples	sample	NOUN
eurjchem-1596	155	2	were	be	AUX
eurjchem-1596	155	3	injected	inject	VERB
eurjchem-1596	155	4	as	as	ADP
eurjchem-1596	155	5	per	per	ADP
eurjchem-1596	155	6	method	method	NOUN
eurjchem-1596	155	7	validation	validation	NOUN
eurjchem-1596	155	8	working	working	NOUN
eurjchem-1596	155	9	plan	plan	NOUN
eurjchem-1596	155	10	.	.	PUNCT
eurjchem-1596	156	1	%	%	INTJ
eurjchem-1596	156	2	stability	stability	NOUN
eurjchem-1596	156	3	was	be	AUX
eurjchem-1596	156	4	indicated	indicate	VERB
eurjchem-1596	156	5	based	base	VERB
eurjchem-1596	156	6	on	on	ADP
eurjchem-1596	156	7	precision	precision	NOUN
eurjchem-1596	156	8	and	and	CCONJ
eurjchem-1596	156	9	accuracy	accuracy	NOUN
eurjchem-1596	156	10	results	result	NOUN
eurjchem-1596	156	11	of	of	ADP
eurjchem-1596	156	12	stability	stability	NOUN
eurjchem-1596	156	13	control	control	NOUN
eurjchem-1596	156	14	samples	sample	NOUN
eurjchem-1596	156	15	.	.	PUNCT
eurjchem-1596	157	1	pappula	pappula	PROPN
eurjchem-1596	157	2	et	et	PROPN
eurjchem-1596	157	3	al	al	PROPN
eurjchem-1596	157	4	.	.	PUNCT
eurjchem-1596	157	5	/	/	SYM
eurjchem-1596	157	6	european	european	PROPN
eurjchem-1596	157	7	journal	journal	PROPN
eurjchem-1596	157	8	of	of	ADP
eurjchem-1596	157	9	chemistry	chemistry	NOUN
eurjchem-1596	157	10	8	8	NUM
eurjchem-1596	157	11	(	(	PUNCT
eurjchem-1596	157	12	3	3	NUM
eurjchem-1596	157	13	)	)	PUNCT
eurjchem-1596	157	14	(	(	PUNCT
eurjchem-1596	157	15	2017	2017	NUM
eurjchem-1596	157	16	)	)	PUNCT
eurjchem-1596	157	17	258‐264	258‐264	NOUN
eurjchem-1596	157	18	263	263	NUM
eurjchem-1596	157	19	table	table	NOUN
eurjchem-1596	157	20	4	4	NUM
eurjchem-1596	157	21	.	.	PUNCT
eurjchem-1596	158	1	stability	stability	NOUN
eurjchem-1596	158	2	data	datum	NOUN
eurjchem-1596	158	3	of	of	ADP
eurjchem-1596	158	4	ulipristal	ulipristal	ADJ
eurjchem-1596	158	5	acetate	acetate	NOUN
eurjchem-1596	158	6	under	under	ADP
eurjchem-1596	158	7	different	different	ADJ
eurjchem-1596	158	8	conditions	condition	NOUN
eurjchem-1596	158	9	.	.	PUNCT
eurjchem-1596	159	1	stability	stability	NOUN
eurjchem-1596	159	2	conditions	condition	NOUN
eurjchem-1596	159	3	conc	conc	VERB
eurjchem-1596	159	4	.	.	PUNCT
eurjchem-1596	160	1	added	add	VERB
eurjchem-1596	160	2	(	(	PUNCT
eurjchem-1596	160	3	ng	ng	PROPN
eurjchem-1596	160	4	/	/	SYM
eurjchem-1596	160	5	ml	ml	NOUN
eurjchem-1596	160	6	)	)	PUNCT
eurjchem-1596	160	7	stability	stability	NOUN
eurjchem-1596	160	8	(	(	PUNCT
eurjchem-1596	160	9	%	%	INTJ
eurjchem-1596	160	10	)	)	PUNCT
eurjchem-1596	160	11	precision	precision	NOUN
eurjchem-1596	160	12	(	(	PUNCT
eurjchem-1596	160	13	%	%	INTJ
eurjchem-1596	160	14	)	)	PUNCT
eurjchem-1596	160	15	ambient	ambient	ADJ
eurjchem-1596	160	16	temperature	temperature	NOUN
eurjchem-1596	160	17	20.67	20.67	NUM
eurjchem-1596	160	18	h	h	NOUN
eurjchem-1596	160	19	3	3	NUM
eurjchem-1596	160	20	99.3	99.3	NUM
eurjchem-1596	160	21	2.3	2.3	NUM
eurjchem-1596	160	22	228	228	NUM
eurjchem-1596	160	23	98.9	98.9	NUM
eurjchem-1596	160	24	3.0	3.0	NUM
eurjchem-1596	160	25	freeze	freeze	NOUN
eurjchem-1596	160	26	and	and	CCONJ
eurjchem-1596	160	27	thaw	thaw	NOUN
eurjchem-1596	160	28	cycles	cycle	NOUN
eurjchem-1596	160	29	3	3	NUM
eurjchem-1596	160	30	99.1	99.1	NUM
eurjchem-1596	160	31	3.9	3.9	NUM
eurjchem-1596	160	32	228	228	NUM
eurjchem-1596	160	33	97.3	97.3	NUM
eurjchem-1596	160	34	3.2	3.2	NUM
eurjchem-1596	160	35	auto	auto	NOUN
eurjchem-1596	160	36	sampler	sampler	NOUN
eurjchem-1596	160	37	at	at	ADP
eurjchem-1596	160	38	5	5	NUM
eurjchem-1596	160	39	°	°	ADP
eurjchem-1596	160	40	c	c	NOUN
eurjchem-1596	160	41	for	for	ADP
eurjchem-1596	160	42	29	29	NUM
eurjchem-1596	160	43	h	h	NOUN
eurjchem-1596	160	44	3	3	NUM
eurjchem-1596	160	45	97.2	97.2	NUM
eurjchem-1596	160	46	5.1	5.1	NUM
eurjchem-1596	160	47	228	228	NUM
eurjchem-1596	160	48	97.9	97.9	NUM
eurjchem-1596	160	49	2.6	2.6	NUM
eurjchem-1596	160	50	dry	dry	ADJ
eurjchem-1596	160	51	extract	extract	NOUN
eurjchem-1596	160	52	at	at	ADP
eurjchem-1596	160	53	2‐8	2‐8	NOUN
eurjchem-1596	160	54	°	°	ADP
eurjchem-1596	160	55	c	c	NOUN
eurjchem-1596	160	56	for	for	ADP
eurjchem-1596	160	57	35.98	35.98	NUM
eurjchem-1596	160	58	h	h	NOUN
eurjchem-1596	160	59	3	3	NUM
eurjchem-1596	160	60	99.0	99.0	NUM
eurjchem-1596	160	61	3.3	3.3	NUM
eurjchem-1596	160	62	228	228	NUM
eurjchem-1596	160	63	98.0	98.0	NUM
eurjchem-1596	160	64	3.3	3.3	NUM
eurjchem-1596	160	65	long	long	ADJ
eurjchem-1596	160	66	term	term	NOUN
eurjchem-1596	160	67	at	at	ADP
eurjchem-1596	160	68	‐70	‐70	PROPN
eurjchem-1596	160	69	°	°	ADP
eurjchem-1596	160	70	c	c	NOUN
eurjchem-1596	160	71	for	for	ADP
eurjchem-1596	160	72	42	42	NUM
eurjchem-1596	160	73	d	d	SYM
eurjchem-1596	160	74	3	3	NUM
eurjchem-1596	160	75	98.3	98.3	NUM
eurjchem-1596	160	76	4.6	4.6	NUM
eurjchem-1596	160	77	228	228	NUM
eurjchem-1596	160	78	98.1	98.1	NUM
eurjchem-1596	160	79	3.7	3.7	NUM
eurjchem-1596	160	80	the	the	DET
eurjchem-1596	160	81	analyte	analyte	NOUN
eurjchem-1596	160	82	was	be	AUX
eurjchem-1596	160	83	considered	consider	VERB
eurjchem-1596	160	84	to	to	PART
eurjchem-1596	160	85	be	be	AUX
eurjchem-1596	160	86	stable	stable	ADJ
eurjchem-1596	160	87	in	in	ADP
eurjchem-1596	160	88	the	the	DET
eurjchem-1596	160	89	tested	test	VERB
eurjchem-1596	160	90	conditions	condition	NOUN
eurjchem-1596	160	91	if	if	SCONJ
eurjchem-1596	160	92	the	the	DET
eurjchem-1596	160	93	precision	precision	NOUN
eurjchem-1596	160	94	and	and	CCONJ
eurjchem-1596	160	95	accuracy	accuracy	NOUN
eurjchem-1596	160	96	was	be	AUX
eurjchem-1596	160	97	within	within	ADP
eurjchem-1596	160	98	≤15	≤15	NOUN
eurjchem-1596	160	99	%	%	NOUN
eurjchem-1596	160	100	and	and	CCONJ
eurjchem-1596	160	101	±15	±15	NOUN
eurjchem-1596	160	102	%	%	NOUN
eurjchem-1596	160	103	(	(	PUNCT
eurjchem-1596	160	104	85‐115	85‐115	NUM
eurjchem-1596	160	105	%	%	NOUN
eurjchem-1596	160	106	)	)	PUNCT
eurjchem-1596	160	107	,	,	PUNCT
eurjchem-1596	160	108	respectively	respectively	ADV
eurjchem-1596	160	109	.	.	PUNCT
eurjchem-1596	161	1	the	the	DET
eurjchem-1596	161	2	stability	stability	NOUN
eurjchem-1596	161	3	conditions	condition	NOUN
eurjchem-1596	161	4	and	and	CCONJ
eurjchem-1596	161	5	results	result	NOUN
eurjchem-1596	161	6	were	be	AUX
eurjchem-1596	161	7	shown	show	VERB
eurjchem-1596	161	8	in	in	ADP
eurjchem-1596	161	9	table	table	NOUN
eurjchem-1596	161	10	4	4	NUM
eurjchem-1596	161	11	.	.	PUNCT
eurjchem-1596	162	1	(	(	PUNCT
eurjchem-1596	162	2	a	a	X
eurjchem-1596	162	3	)	)	PUNCT
eurjchem-1596	162	4	(	(	PUNCT
eurjchem-1596	162	5	b	b	X
eurjchem-1596	162	6	)	)	PUNCT
eurjchem-1596	162	7	figure	figure	NOUN
eurjchem-1596	162	8	5	5	NUM
eurjchem-1596	162	9	.	.	NOUN
eurjchem-1596	162	10	chromatograms	chromatogram	NOUN
eurjchem-1596	162	11	of	of	ADP
eurjchem-1596	162	12	(	(	PUNCT
eurjchem-1596	162	13	a	a	DET
eurjchem-1596	162	14	)	)	PUNCT
eurjchem-1596	162	15	ulipristal	ulipristal	ADJ
eurjchem-1596	162	16	acetate	acetate	NOUN
eurjchem-1596	162	17	and	and	CCONJ
eurjchem-1596	162	18	(	(	PUNCT
eurjchem-1596	162	19	b	b	NOUN
eurjchem-1596	162	20	)	)	PUNCT
eurjchem-1596	162	21	levonorgestrel	levonorgestrel	NOUN
eurjchem-1596	162	22	at	at	ADP
eurjchem-1596	162	23	uloq	uloq	PROPN
eurjchem-1596	162	24	level	level	NOUN
eurjchem-1596	162	25	.	.	PUNCT
eurjchem-1596	163	1	3.2.10	3.2.10	NUM
eurjchem-1596	163	2	.	.	PUNCT
eurjchem-1596	164	1	stability	stability	NOUN
eurjchem-1596	164	2	in	in	ADP
eurjchem-1596	164	3	solutions	solution	NOUN
eurjchem-1596	164	4	stock	stock	NOUN
eurjchem-1596	164	5	solution	solution	NOUN
eurjchem-1596	164	6	and	and	CCONJ
eurjchem-1596	164	7	working	working	NOUN
eurjchem-1596	164	8	solution	solution	NOUN
eurjchem-1596	164	9	stability	stability	NOUN
eurjchem-1596	164	10	was	be	AUX
eurjchem-1596	164	11	assessed	assess	VERB
eurjchem-1596	164	12	at	at	ADP
eurjchem-1596	164	13	room	room	NOUN
eurjchem-1596	164	14	temperature	temperature	NOUN
eurjchem-1596	164	15	(	(	PUNCT
eurjchem-1596	164	16	after	after	ADP
eurjchem-1596	164	17	8	8	NUM
eurjchem-1596	164	18	to	to	PART
eurjchem-1596	164	19	10	10	NUM
eurjchem-1596	164	20	hours	hour	NOUN
eurjchem-1596	164	21	)	)	PUNCT
eurjchem-1596	164	22	and	and	CCONJ
eurjchem-1596	164	23	in	in	ADP
eurjchem-1596	164	24	refrigerator	refrigerator	NOUN
eurjchem-1596	164	25	at	at	ADP
eurjchem-1596	164	26	2‐8	2‐8	NOUN
eurjchem-1596	164	27	°	°	ADP
eurjchem-1596	164	28	c	c	NOUN
eurjchem-1596	164	29	after	after	ADP
eurjchem-1596	164	30	six	six	NUM
eurjchem-1596	164	31	days	day	NOUN
eurjchem-1596	164	32	.	.	PUNCT
eurjchem-1596	165	1	the	the	DET
eurjchem-1596	165	2	%	%	NOUN
eurjchem-1596	165	3	stability	stability	NOUN
eurjchem-1596	165	4	was	be	AUX
eurjchem-1596	165	5	calculated	calculate	VERB
eurjchem-1596	165	6	by	by	ADP
eurjchem-1596	165	7	comparing	compare	VERB
eurjchem-1596	165	8	mean	mean	ADJ
eurjchem-1596	165	9	response	response	NOUN
eurjchem-1596	165	10	of	of	ADP
eurjchem-1596	165	11	six	six	NUM
eurjchem-1596	165	12	replicates	replicate	NOUN
eurjchem-1596	165	13	of	of	ADP
eurjchem-1596	165	14	stability	stability	NOUN
eurjchem-1596	165	15	and	and	CCONJ
eurjchem-1596	165	16	comparison	comparison	NOUN
eurjchem-1596	165	17	samples	sample	NOUN
eurjchem-1596	165	18	.	.	PUNCT
eurjchem-1596	166	1	the	the	DET
eurjchem-1596	166	2	stock	stock	NOUN
eurjchem-1596	166	3	solutions	solution	NOUN
eurjchem-1596	166	4	and	and	CCONJ
eurjchem-1596	166	5	working	working	NOUN
eurjchem-1596	166	6	dilutions	dilution	NOUN
eurjchem-1596	166	7	were	be	AUX
eurjchem-1596	166	8	stable	stable	ADJ
eurjchem-1596	166	9	at	at	ADP
eurjchem-1596	166	10	proposed	propose	VERB
eurjchem-1596	166	11	conditions	condition	NOUN
eurjchem-1596	166	12	.	.	PUNCT
eurjchem-1596	167	1	3.2.11	3.2.11	X
eurjchem-1596	167	2	.	.	PUNCT
eurjchem-1596	167	3	concomitant	concomitant	ADJ
eurjchem-1596	167	4	medication	medication	NOUN
eurjchem-1596	167	5	during	during	ADP
eurjchem-1596	167	6	clinical	clinical	ADJ
eurjchem-1596	167	7	trial	trial	NOUN
eurjchem-1596	167	8	process	process	NOUN
eurjchem-1596	167	9	,	,	PUNCT
eurjchem-1596	167	10	investigators	investigator	NOUN
eurjchem-1596	167	11	may	may	AUX
eurjchem-1596	167	12	use	use	VERB
eurjchem-1596	167	13	some	some	PRON
eurjchem-1596	167	14	over	over	ADP
eurjchem-1596	167	15	the	the	DET
eurjchem-1596	167	16	counter	counter	ADJ
eurjchem-1596	167	17	medications	medication	NOUN
eurjchem-1596	167	18	to	to	PART
eurjchem-1596	167	19	treat	treat	VERB
eurjchem-1596	167	20	unexpected	unexpected	ADJ
eurjchem-1596	167	21	or	or	CCONJ
eurjchem-1596	167	22	expected	expect	VERB
eurjchem-1596	167	23	adverse	adverse	ADJ
eurjchem-1596	167	24	effects	effect	NOUN
eurjchem-1596	167	25	like	like	ADP
eurjchem-1596	167	26	fever	fever	NOUN
eurjchem-1596	167	27	,	,	PUNCT
eurjchem-1596	167	28	nausea	nausea	NOUN
eurjchem-1596	167	29	,	,	PUNCT
eurjchem-1596	167	30	vomiting	vomiting	NOUN
eurjchem-1596	167	31	etc	etc	X
eurjchem-1596	167	32	.	.	X
eurjchem-1596	168	1	therefore	therefore	ADV
eurjchem-1596	168	2	,	,	PUNCT
eurjchem-1596	168	3	selectivity	selectivity	NOUN
eurjchem-1596	168	4	and	and	CCONJ
eurjchem-1596	168	5	reproducibility	reproducibility	NOUN
eurjchem-1596	168	6	of	of	ADP
eurjchem-1596	168	7	the	the	DET
eurjchem-1596	168	8	analytical	analytical	ADJ
eurjchem-1596	168	9	method	method	NOUN
eurjchem-1596	168	10	was	be	AUX
eurjchem-1596	168	11	evaluated	evaluate	VERB
eurjchem-1596	168	12	in	in	ADP
eurjchem-1596	168	13	presence	presence	NOUN
eurjchem-1596	168	14	of	of	ADP
eurjchem-1596	168	15	concomitant	concomitant	ADJ
eurjchem-1596	168	16	drugs	drug	NOUN
eurjchem-1596	168	17	by	by	ADP
eurjchem-1596	168	18	spiking	spike	VERB
eurjchem-1596	168	19	respective	respective	ADJ
eurjchem-1596	168	20	drug	drug	NOUN
eurjchem-1596	168	21	dilutions	dilution	NOUN
eurjchem-1596	168	22	in	in	ADP
eurjchem-1596	168	23	individual	individual	ADJ
eurjchem-1596	168	24	blank	blank	ADJ
eurjchem-1596	168	25	plasma	plasma	NOUN
eurjchem-1596	168	26	samples	sample	NOUN
eurjchem-1596	168	27	.	.	PUNCT
eurjchem-1596	169	1	along	along	ADP
eurjchem-1596	169	2	with	with	ADP
eurjchem-1596	169	3	this	this	DET
eurjchem-1596	169	4	cocktail	cocktail	NOUN
eurjchem-1596	169	5	mixture	mixture	NOUN
eurjchem-1596	169	6	of	of	ADP
eurjchem-1596	169	7	concomitant	concomitant	ADJ
eurjchem-1596	169	8	drug	drug	NOUN
eurjchem-1596	169	9	dilution	dilution	NOUN
eurjchem-1596	169	10	was	be	AUX
eurjchem-1596	169	11	prepared	prepare	VERB
eurjchem-1596	169	12	and	and	CCONJ
eurjchem-1596	169	13	spiked	spike	VERB
eurjchem-1596	169	14	at	at	ADP
eurjchem-1596	169	15	lqc	lqc	ADJ
eurjchem-1596	169	16	level	level	NOUN
eurjchem-1596	169	17	.	.	PUNCT
eurjchem-1596	170	1	the	the	DET
eurjchem-1596	170	2	concentration	concentration	NOUN
eurjchem-1596	170	3	of	of	ADP
eurjchem-1596	170	4	concomitant	concomitant	ADJ
eurjchem-1596	170	5	medication	medication	NOUN
eurjchem-1596	170	6	drugs	drug	NOUN
eurjchem-1596	170	7	used	use	VERB
eurjchem-1596	170	8	approximately	approximately	ADV
eurjchem-1596	170	9	equal	equal	ADJ
eurjchem-1596	170	10	to	to	ADP
eurjchem-1596	170	11	their	their	PRON
eurjchem-1596	170	12	cmax	cmax	NOUN
eurjchem-1596	170	13	value	value	NOUN
eurjchem-1596	170	14	.	.	PUNCT
eurjchem-1596	171	1	prepared	prepare	VERB
eurjchem-1596	171	2	samples	sample	NOUN
eurjchem-1596	171	3	were	be	AUX
eurjchem-1596	171	4	subjected	subject	VERB
eurjchem-1596	171	5	to	to	ADP
eurjchem-1596	171	6	extraction	extraction	NOUN
eurjchem-1596	171	7	along	along	ADP
eurjchem-1596	171	8	with	with	ADP
eurjchem-1596	171	9	calibration	calibration	NOUN
eurjchem-1596	171	10	curve	curve	NOUN
eurjchem-1596	171	11	and	and	CCONJ
eurjchem-1596	171	12	analysed	analyse	VERB
eurjchem-1596	171	13	.	.	PUNCT
eurjchem-1596	172	1	the	the	DET
eurjchem-1596	172	2	precision	precision	NOUN
eurjchem-1596	172	3	and	and	CCONJ
eurjchem-1596	172	4	accuracy	accuracy	NOUN
eurjchem-1596	172	5	of	of	ADP
eurjchem-1596	172	6	lqc	lqc	ADJ
eurjchem-1596	172	7	samples	sample	NOUN
eurjchem-1596	172	8	and	and	CCONJ
eurjchem-1596	172	9	observed	observe	VERB
eurjchem-1596	172	10	interference	interference	NOUN
eurjchem-1596	172	11	from	from	ADP
eurjchem-1596	172	12	blank	blank	ADJ
eurjchem-1596	172	13	samples	sample	NOUN
eurjchem-1596	172	14	at	at	ADP
eurjchem-1596	172	15	retention	retention	NOUN
eurjchem-1596	172	16	time	time	NOUN
eurjchem-1596	172	17	of	of	ADP
eurjchem-1596	172	18	analyte	analyte	NOUN
eurjchem-1596	172	19	and	and	CCONJ
eurjchem-1596	172	20	istd	istd	NOUN
eurjchem-1596	172	21	compared	compare	VERB
eurjchem-1596	172	22	to	to	ADP
eurjchem-1596	172	23	low	low	ADJ
eurjchem-1596	172	24	standard	standard	NOUN
eurjchem-1596	172	25	in	in	ADP
eurjchem-1596	172	26	calibration	calibration	NOUN
eurjchem-1596	172	27	curve	curve	NOUN
eurjchem-1596	172	28	were	be	AUX
eurjchem-1596	172	29	found	find	VERB
eurjchem-1596	172	30	to	to	PART
eurjchem-1596	172	31	be	be	AUX
eurjchem-1596	172	32	within	within	ADP
eurjchem-1596	172	33	acceptable	acceptable	ADJ
eurjchem-1596	172	34	limits	limit	NOUN
eurjchem-1596	172	35	.	.	PUNCT
eurjchem-1596	173	1	the	the	DET
eurjchem-1596	173	2	commonly	commonly	ADV
eurjchem-1596	173	3	used	use	VERB
eurjchem-1596	173	4	drugs	drug	NOUN
eurjchem-1596	173	5	as	as	ADP
eurjchem-1596	173	6	per	per	ADP
eurjchem-1596	173	7	method	method	NOUN
eurjchem-1596	173	8	validation	validation	NOUN
eurjchem-1596	173	9	plan	plan	NOUN
eurjchem-1596	173	10	are	be	AUX
eurjchem-1596	173	11	paracetamol	paracetamol	NOUN
eurjchem-1596	173	12	,	,	PUNCT
eurjchem-1596	173	13	ibuprofen	ibuprofen	NOUN
eurjchem-1596	173	14	,	,	PUNCT
eurjchem-1596	173	15	aceclofenac	aceclofenac	PROPN
eurjchem-1596	173	16	,	,	PUNCT
eurjchem-1596	173	17	ranitidine	ranitidine	NOUN
eurjchem-1596	173	18	and	and	CCONJ
eurjchem-1596	173	19	ondansetron	ondansetron	NOUN
eurjchem-1596	173	20	.	.	PUNCT
eurjchem-1596	174	1	3.2.12	3.2.12	NUM
eurjchem-1596	174	2	.	.	PUNCT
eurjchem-1596	175	1	whole	whole	ADJ
eurjchem-1596	175	2	human	human	ADJ
eurjchem-1596	175	3	blood	blood	NOUN
eurjchem-1596	175	4	stability	stability	NOUN
eurjchem-1596	175	5	stability	stability	NOUN
eurjchem-1596	175	6	of	of	ADP
eurjchem-1596	175	7	the	the	DET
eurjchem-1596	175	8	analyte	analyte	NOUN
eurjchem-1596	175	9	in	in	ADP
eurjchem-1596	175	10	whole	whole	ADJ
eurjchem-1596	175	11	human	human	ADJ
eurjchem-1596	175	12	blood	blood	NOUN
eurjchem-1596	175	13	was	be	AUX
eurjchem-1596	175	14	evaluated	evaluate	VERB
eurjchem-1596	175	15	at	at	ADP
eurjchem-1596	175	16	room	room	NOUN
eurjchem-1596	175	17	temperature	temperature	NOUN
eurjchem-1596	175	18	.	.	PUNCT
eurjchem-1596	176	1	stability	stability	NOUN
eurjchem-1596	176	2	samples	sample	NOUN
eurjchem-1596	176	3	at	at	ADP
eurjchem-1596	176	4	lqc	lqc	NOUN
eurjchem-1596	176	5	and	and	CCONJ
eurjchem-1596	176	6	hqc	hqc	ADJ
eurjchem-1596	176	7	level	level	NOUN
eurjchem-1596	176	8	in	in	ADP
eurjchem-1596	176	9	whole	whole	ADJ
eurjchem-1596	176	10	human	human	ADJ
eurjchem-1596	176	11	blood	blood	NOUN
eurjchem-1596	176	12	were	be	AUX
eurjchem-1596	176	13	prepared	prepare	VERB
eurjchem-1596	176	14	and	and	CCONJ
eurjchem-1596	176	15	kept	keep	VERB
eurjchem-1596	176	16	on	on	ADP
eurjchem-1596	176	17	the	the	DET
eurjchem-1596	176	18	working	work	VERB
eurjchem-1596	176	19	bench	bench	NOUN
eurjchem-1596	176	20	.	.	PUNCT
eurjchem-1596	177	1	approximately	approximately	ADV
eurjchem-1596	177	2	after	after	ADP
eurjchem-1596	177	3	2	2	NUM
eurjchem-1596	177	4	hr	hr	NOUN
eurjchem-1596	177	5	.	.	PUNCT
eurjchem-1596	177	6	,	,	PUNCT
eurjchem-1596	177	7	comparison	comparison	NOUN
eurjchem-1596	177	8	samples	sample	NOUN
eurjchem-1596	177	9	were	be	AUX
eurjchem-1596	177	10	also	also	ADV
eurjchem-1596	177	11	prepared	prepare	VERB
eurjchem-1596	177	12	in	in	ADP
eurjchem-1596	177	13	whole	whole	ADJ
eurjchem-1596	177	14	human	human	ADJ
eurjchem-1596	177	15	blood	blood	NOUN
eurjchem-1596	177	16	.	.	PUNCT
eurjchem-1596	178	1	plasma	plasma	NOUN
eurjchem-1596	178	2	was	be	AUX
eurjchem-1596	178	3	separated	separate	VERB
eurjchem-1596	178	4	from	from	ADP
eurjchem-1596	178	5	both	both	DET
eurjchem-1596	178	6	comparison	comparison	NOUN
eurjchem-1596	178	7	and	and	CCONJ
eurjchem-1596	178	8	stability	stability	NOUN
eurjchem-1596	178	9	samples	sample	NOUN
eurjchem-1596	178	10	by	by	ADP
eurjchem-1596	178	11	centrifuging	centrifuge	VERB
eurjchem-1596	178	12	the	the	DET
eurjchem-1596	178	13	samples	sample	NOUN
eurjchem-1596	178	14	at	at	ADP
eurjchem-1596	178	15	3000	3000	NUM
eurjchem-1596	178	16	rpm	rpm	NOUN
eurjchem-1596	178	17	at	at	ADP
eurjchem-1596	178	18	4	4	NUM
eurjchem-1596	178	19	°	°	NOUN
eurjchem-1596	178	20	c	c	NOUN
eurjchem-1596	178	21	for	for	ADP
eurjchem-1596	178	22	about	about	ADV
eurjchem-1596	178	23	20	20	NUM
eurjchem-1596	178	24	min	min	NOUN
eurjchem-1596	178	25	.	.	PUNCT
eurjchem-1596	179	1	each	each	DET
eurjchem-1596	179	2	six	six	NUM
eurjchem-1596	179	3	replicates	replicate	NOUN
eurjchem-1596	179	4	lqc	lqc	ADJ
eurjchem-1596	179	5	and	and	CCONJ
eurjchem-1596	179	6	hqc	hqc	ADP
eurjchem-1596	179	7	level	level	NOUN
eurjchem-1596	179	8	from	from	ADP
eurjchem-1596	179	9	both	both	CCONJ
eurjchem-1596	179	10	stability	stability	NOUN
eurjchem-1596	179	11	and	and	CCONJ
eurjchem-1596	179	12	comparison	comparison	NOUN
eurjchem-1596	179	13	samples	sample	NOUN
eurjchem-1596	179	14	were	be	AUX
eurjchem-1596	179	15	processed	process	VERB
eurjchem-1596	179	16	as	as	ADP
eurjchem-1596	179	17	per	per	ADP
eurjchem-1596	179	18	sample	sample	NOUN
eurjchem-1596	179	19	extraction	extraction	NOUN
eurjchem-1596	179	20	procedure	procedure	NOUN
eurjchem-1596	179	21	and	and	CCONJ
eurjchem-1596	179	22	analysed	analyse	VERB
eurjchem-1596	179	23	.	.	PUNCT
eurjchem-1596	180	1	the	the	DET
eurjchem-1596	180	2	percentage	percentage	NOUN
eurjchem-1596	180	3	stability	stability	NOUN
eurjchem-1596	180	4	was	be	AUX
eurjchem-1596	180	5	calculated	calculate	VERB
eurjchem-1596	180	6	by	by	ADP
eurjchem-1596	180	7	comparing	compare	VERB
eurjchem-1596	180	8	the	the	DET
eurjchem-1596	180	9	mean	mean	ADJ
eurjchem-1596	180	10	area	area	NOUN
eurjchem-1596	180	11	ratios	ratio	NOUN
eurjchem-1596	180	12	of	of	ADP
eurjchem-1596	180	13	stability	stability	NOUN
eurjchem-1596	180	14	and	and	CCONJ
eurjchem-1596	180	15	comparison	comparison	NOUN
eurjchem-1596	180	16	samples	sample	NOUN
eurjchem-1596	180	17	at	at	ADP
eurjchem-1596	180	18	lqc	lqc	NOUN
eurjchem-1596	180	19	and	and	CCONJ
eurjchem-1596	180	20	hqc	hqc	PROPN
eurjchem-1596	180	21	levels	level	NOUN
eurjchem-1596	180	22	.	.	PUNCT
eurjchem-1596	181	1	the	the	DET
eurjchem-1596	181	2	%	%	NOUN
eurjchem-1596	181	3	stability	stability	NOUN
eurjchem-1596	181	4	and	and	CCONJ
eurjchem-1596	181	5	precision	precision	NOUN
eurjchem-1596	181	6	at	at	ADP
eurjchem-1596	181	7	lqc	lqc	NOUN
eurjchem-1596	181	8	and	and	CCONJ
eurjchem-1596	181	9	hqc	hqc	PROPN
eurjchem-1596	181	10	were	be	AUX
eurjchem-1596	181	11	93.5	93.5	NUM
eurjchem-1596	181	12	%	%	NOUN
eurjchem-1596	181	13	,	,	PUNCT
eurjchem-1596	181	14	1.8	1.8	NUM
eurjchem-1596	181	15	,	,	PUNCT
eurjchem-1596	181	16	and	and	CCONJ
eurjchem-1596	181	17	96.4	96.4	NUM
eurjchem-1596	181	18	%	%	NOUN
eurjchem-1596	181	19	,	,	PUNCT
eurjchem-1596	181	20	0.6	0.6	NUM
eurjchem-1596	181	21	,	,	PUNCT
eurjchem-1596	181	22	respectively	respectively	ADV
eurjchem-1596	181	23	.	.	PUNCT
eurjchem-1596	182	1	3.2.13	3.2.13	NUM
eurjchem-1596	182	2	.	.	NOUN
eurjchem-1596	182	3	extended	extend	VERB
eurjchem-1596	182	4	run	run	NOUN
eurjchem-1596	182	5	(	(	PUNCT
eurjchem-1596	182	6	batch	batch	NOUN
eurjchem-1596	182	7	size	size	NOUN
eurjchem-1596	182	8	)	)	PUNCT
eurjchem-1596	182	9	precision	precision	NOUN
eurjchem-1596	182	10	and	and	CCONJ
eurjchem-1596	182	11	accuracy	accuracy	NOUN
eurjchem-1596	183	1	it	it	PRON
eurjchem-1596	183	2	is	be	AUX
eurjchem-1596	183	3	evaluated	evaluate	VERB
eurjchem-1596	183	4	by	by	ADP
eurjchem-1596	183	5	processing	process	VERB
eurjchem-1596	183	6	three	three	NUM
eurjchem-1596	183	7	control	control	NOUN
eurjchem-1596	183	8	samples	sample	NOUN
eurjchem-1596	183	9	on	on	ADP
eurjchem-1596	183	10	each	each	DET
eurjchem-1596	183	11	level	level	NOUN
eurjchem-1596	183	12	(	(	PUNCT
eurjchem-1596	183	13	lqc	lqc	PROPN
eurjchem-1596	183	14	,	,	PUNCT
eurjchem-1596	183	15	mqc	mqc	PROPN
eurjchem-1596	183	16	,	,	PUNCT
eurjchem-1596	183	17	hqc	hqc	PROPN
eurjchem-1596	183	18	)	)	PUNCT
eurjchem-1596	183	19	from	from	ADP
eurjchem-1596	183	20	six	six	NUM
eurjchem-1596	183	21	different	different	ADJ
eurjchem-1596	183	22	plasma	plasma	NOUN
eurjchem-1596	183	23	vacutainer	vacutainer	ADJ
eurjchem-1596	183	24	sources	source	NOUN
eurjchem-1596	183	25	of	of	ADP
eurjchem-1596	183	26	k2	k2	PROPN
eurjchem-1596	183	27	edta	edta	PROPN
eurjchem-1596	183	28	(	(	PUNCT
eurjchem-1596	183	29	jindal	jindal	PROPN
eurjchem-1596	183	30	bio	bio	PROPN
eurjchem-1596	183	31	lab	lab	PROPN
eurjchem-1596	183	32	,	,	PUNCT
eurjchem-1596	183	33	bio	bio	NOUN
eurjchem-1596	183	34	x	x	PROPN
eurjchem-1596	183	35	,	,	PUNCT
eurjchem-1596	183	36	jn	jn	PROPN
eurjchem-1596	183	37	science	science	PROPN
eurjchem-1596	183	38	tech	tech	PROPN
eurjchem-1596	183	39	,	,	PUNCT
eurjchem-1596	183	40	bd‐	bd‐	PRON
eurjchem-1596	183	41	mumbai	mumbai	PROPN
eurjchem-1596	183	42	,	,	PUNCT
eurjchem-1596	183	43	sv	sv	INTJ
eurjchem-1596	183	44	lab	lab	PROPN
eurjchem-1596	183	45	tech‐hyderabad	tech‐hyderabad	PROPN
eurjchem-1596	183	46	,	,	PUNCT
eurjchem-1596	183	47	jai	jai	PROPN
eurjchem-1596	183	48	bro	bro	NOUN
eurjchem-1596	183	49	diagnostics‐delhi	diagnostics‐delhi	PROPN
eurjchem-1596	183	50	)	)	PUNCT
eurjchem-1596	183	51	,	,	PUNCT
eurjchem-1596	183	52	one	one	NUM
eurjchem-1596	183	53	lot	lot	NOUN
eurjchem-1596	183	54	of	of	ADP
eurjchem-1596	183	55	plasma	plasma	NOUN
eurjchem-1596	183	56	pool	pool	NOUN
eurjchem-1596	183	57	(	(	PUNCT
eurjchem-1596	183	58	prepared	prepare	VERB
eurjchem-1596	183	59	from	from	ADP
eurjchem-1596	183	60	screened	screen	VERB
eurjchem-1596	183	61	lots	lot	NOUN
eurjchem-1596	183	62	in	in	ADP
eurjchem-1596	183	63	selectivity	selectivity	NOUN
eurjchem-1596	183	64	)	)	PUNCT
eurjchem-1596	183	65	along	along	ADP
eurjchem-1596	183	66	with	with	ADP
eurjchem-1596	183	67	each	each	DET
eurjchem-1596	183	68	two	two	NUM
eurjchem-1596	183	69	lots	lot	NOUN
eurjchem-1596	183	70	of	of	ADP
eurjchem-1596	183	71	lipemic	lipemic	ADJ
eurjchem-1596	183	72	and	and	CCONJ
eurjchem-1596	183	73	haemolytic	haemolytic	ADJ
eurjchem-1596	183	74	plasma	plasma	NOUN
eurjchem-1596	183	75	.	.	PUNCT
eurjchem-1596	184	1	before	before	ADP
eurjchem-1596	184	2	spiking	spike	VERB
eurjchem-1596	184	3	,	,	PUNCT
eurjchem-1596	184	4	one	one	NUM
eurjchem-1596	184	5	aliquot	aliquot	NOUN
eurjchem-1596	184	6	of	of	ADP
eurjchem-1596	184	7	plasma	plasma	NOUN
eurjchem-1596	184	8	sample	sample	NOUN
eurjchem-1596	184	9	was	be	AUX
eurjchem-1596	184	10	used	use	VERB
eurjchem-1596	184	11	to	to	PART
eurjchem-1596	184	12	screen	screen	VERB
eurjchem-1596	184	13	the	the	DET
eurjchem-1596	184	14	plasma	plasma	NOUN
eurjchem-1596	184	15	lots	lot	NOUN
eurjchem-1596	184	16	.	.	PUNCT
eurjchem-1596	185	1	the	the	DET
eurjchem-1596	185	2	processed	process	VERB
eurjchem-1596	185	3	control	control	NOUN
eurjchem-1596	185	4	samples	sample	NOUN
eurjchem-1596	185	5	were	be	AUX
eurjchem-1596	185	6	analysed	analyse	VERB
eurjchem-1596	185	7	against	against	ADP
eurjchem-1596	185	8	the	the	DET
eurjchem-1596	185	9	calibration	calibration	NOUN
eurjchem-1596	185	10	curve	curve	NOUN
eurjchem-1596	185	11	.	.	PUNCT
eurjchem-1596	186	1	the	the	DET
eurjchem-1596	186	2	overall	overall	ADJ
eurjchem-1596	186	3	accuracy	accuracy	NOUN
eurjchem-1596	186	4	and	and	CCONJ
eurjchem-1596	186	5	precision	precision	NOUN
eurjchem-1596	186	6	at	at	ADP
eurjchem-1596	186	7	lqc	lqc	NOUN
eurjchem-1596	186	8	95.8	95.8	NUM
eurjchem-1596	186	9	,	,	PUNCT
eurjchem-1596	186	10	8.4	8.4	NUM
eurjchem-1596	186	11	%	%	NOUN
eurjchem-1596	186	12	,	,	PUNCT
eurjchem-1596	186	13	mqc	mqc	PROPN
eurjchem-1596	186	14	101.2	101.2	NUM
eurjchem-1596	186	15	%	%	NOUN
eurjchem-1596	186	16	,	,	PUNCT
eurjchem-1596	186	17	5.3	5.3	NUM
eurjchem-1596	186	18	%	%	NOUN
eurjchem-1596	186	19	and	and	CCONJ
eurjchem-1596	186	20	at	at	ADP
eurjchem-1596	186	21	hqc	hqc	NUM
eurjchem-1596	186	22	were	be	AUX
eurjchem-1596	186	23	103	103	NUM
eurjchem-1596	186	24	,	,	PUNCT
eurjchem-1596	186	25	3.4	3.4	NUM
eurjchem-1596	186	26	%	%	NOUN
eurjchem-1596	186	27	.	.	PUNCT
eurjchem-1596	187	1	the	the	DET
eurjchem-1596	187	2	results	result	NOUN
eurjchem-1596	187	3	of	of	ADP
eurjchem-1596	187	4	this	this	DET
eurjchem-1596	187	5	experiment	experiment	NOUN
eurjchem-1596	187	6	shown	show	VERB
eurjchem-1596	187	7	that	that	SCONJ
eurjchem-1596	187	8	the	the	DET
eurjchem-1596	187	9	proposed	propose	VERB
eurjchem-1596	187	10	method	method	NOUN
eurjchem-1596	187	11	was	be	AUX
eurjchem-1596	187	12	suitable	suitable	ADJ
eurjchem-1596	187	13	for	for	ADP
eurjchem-1596	187	14	quantification	quantification	NOUN
eurjchem-1596	187	15	of	of	ADP
eurjchem-1596	187	16	ulipristal	ulipristal	ADJ
eurjchem-1596	187	17	acetate	acetate	NOUN
eurjchem-1596	187	18	in	in	ADP
eurjchem-1596	187	19	clinical	clinical	ADJ
eurjchem-1596	187	20	samples	sample	NOUN
eurjchem-1596	187	21	by	by	ADP
eurjchem-1596	187	22	eliminating	eliminate	VERB
eurjchem-1596	187	23	inter	inter	ADJ
eurjchem-1596	187	24	subject	subject	ADJ
eurjchem-1596	187	25	biological	biological	ADJ
eurjchem-1596	187	26	matrix	matrix	NOUN
eurjchem-1596	187	27	variation	variation	NOUN
eurjchem-1596	187	28	.	.	PUNCT
eurjchem-1596	188	1	the	the	DET
eurjchem-1596	188	2	total	total	ADJ
eurjchem-1596	188	3	number	number	NOUN
eurjchem-1596	188	4	of	of	ADP
eurjchem-1596	188	5	control	control	NOUN
eurjchem-1596	188	6	samples	sample	NOUN
eurjchem-1596	188	7	processed	process	VERB
eurjchem-1596	188	8	was	be	AUX
eurjchem-1596	188	9	more	more	ADJ
eurjchem-1596	188	10	than	than	ADP
eurjchem-1596	188	11	the	the	DET
eurjchem-1596	188	12	total	total	ADJ
eurjchem-1596	188	13	expected	expect	VERB
eurjchem-1596	188	14	sampling	sampling	NOUN
eurjchem-1596	188	15	time	time	NOUN
eurjchem-1596	188	16	points	point	NOUN
eurjchem-1596	188	17	for	for	ADP
eurjchem-1596	188	18	human	human	ADJ
eurjchem-1596	188	19	pharmacokinetics	pharmacokinetic	NOUN
eurjchem-1596	188	20	/	/	SYM
eurjchem-1596	188	21	bioequivalence	bioequivalence	NOUN
eurjchem-1596	188	22	studies	study	NOUN
eurjchem-1596	188	23	of	of	ADP
eurjchem-1596	188	24	ulipristal	ulipristal	ADJ
eurjchem-1596	188	25	acetate	acetate	NOUN
eurjchem-1596	188	26	.	.	PUNCT
eurjchem-1596	189	1	the	the	DET
eurjchem-1596	189	2	expected	expect	VERB
eurjchem-1596	189	3	samples	sample	NOUN
eurjchem-1596	189	4	were	be	AUX
eurjchem-1596	189	5	considered	consider	VERB
eurjchem-1596	189	6	based	base	VERB
eurjchem-1596	189	7	on	on	ADP
eurjchem-1596	189	8	the	the	DET
eurjchem-1596	189	9	pharma‐	pharma‐	NOUN
eurjchem-1596	189	10	cokinetic	cokinetic	ADJ
eurjchem-1596	189	11	data	datum	NOUN
eurjchem-1596	189	12	of	of	ADP
eurjchem-1596	189	13	ulipristal	ulipristal	ADJ
eurjchem-1596	189	14	acetate	acetate	NOUN
eurjchem-1596	190	1	[	[	X
eurjchem-1596	190	2	13	13	NUM
eurjchem-1596	190	3	]	]	PUNCT
eurjchem-1596	190	4	.	.	PUNCT
eurjchem-1596	191	1	the	the	DET
eurjchem-1596	191	2	control	control	NOUN
eurjchem-1596	191	3	samples	sample	VERB
eurjchem-1596	191	4	acceptance	acceptance	NOUN
eurjchem-1596	191	5	in	in	ADP
eurjchem-1596	191	6	extended	extended	ADJ
eurjchem-1596	191	7	precision	precision	NOUN
eurjchem-1596	191	8	and	and	CCONJ
eurjchem-1596	191	9	accuracy	accuracy	NOUN
eurjchem-1596	191	10	run	run	NOUN
eurjchem-1596	191	11	indicates	indicate	VERB
eurjchem-1596	191	12	that	that	DET
eurjchem-1596	191	13	method	method	NOUN
eurjchem-1596	191	14	was	be	AUX
eurjchem-1596	191	15	reproducible	reproducible	ADJ
eurjchem-1596	191	16	and	and	CCONJ
eurjchem-1596	191	17	precise	precise	ADJ
eurjchem-1596	191	18	for	for	ADP
eurjchem-1596	191	19	a	a	DET
eurjchem-1596	191	20	complete	complete	ADJ
eurjchem-1596	191	21	analytical	analytical	ADJ
eurjchem-1596	191	22	batch	batch	NOUN
eurjchem-1596	191	23	run	run	VERB
eurjchem-1596	191	24	under	under	ADP
eurjchem-1596	191	25	regulated	regulated	ADJ
eurjchem-1596	191	26	environment	environment	NOUN
eurjchem-1596	191	27	.	.	PUNCT
eurjchem-1596	192	1	3.2.13.1	3.2.13.1	X
eurjchem-1596	192	2	.	.	PUNCT
eurjchem-1596	192	3	istd	istd	NOUN
eurjchem-1596	192	4	trend	trend	NOUN
eurjchem-1596	192	5	analysis	analysis	NOUN
eurjchem-1596	192	6	the	the	DET
eurjchem-1596	192	7	variation	variation	NOUN
eurjchem-1596	192	8	in	in	ADP
eurjchem-1596	192	9	istd	istd	NOUN
eurjchem-1596	192	10	response	response	NOUN
eurjchem-1596	192	11	will	will	AUX
eurjchem-1596	192	12	affect	affect	VERB
eurjchem-1596	192	13	the	the	DET
eurjchem-1596	192	14	unknown	unknown	ADJ
eurjchem-1596	192	15	sample	sample	NOUN
eurjchem-1596	192	16	concentrations	concentration	NOUN
eurjchem-1596	192	17	.	.	PUNCT
eurjchem-1596	193	1	istd	istd	NOUN
eurjchem-1596	193	2	variation	variation	NOUN
eurjchem-1596	193	3	was	be	AUX
eurjchem-1596	193	4	calculated	calculate	VERB
eurjchem-1596	193	5	for	for	ADP
eurjchem-1596	193	6	each	each	DET
eurjchem-1596	193	7	individual	individual	ADJ
eurjchem-1596	193	8	analytical	analytical	ADJ
eurjchem-1596	193	9	run	run	NOUN
eurjchem-1596	193	10	by	by	ADP
eurjchem-1596	193	11	calculating	calculate	VERB
eurjchem-1596	193	12	the	the	DET
eurjchem-1596	193	13	average	average	ADJ
eurjchem-1596	193	14	response	response	NOUN
eurjchem-1596	193	15	area	area	NOUN
eurjchem-1596	193	16	of	of	ADP
eurjchem-1596	193	17	accepted	accept	VERB
eurjchem-1596	193	18	calibration	calibration	NOUN
eurjchem-1596	193	19	curve	curve	NOUN
eurjchem-1596	193	20	and	and	CCONJ
eurjchem-1596	193	21	control	control	NOUN
eurjchem-1596	193	22	samples	sample	NOUN
eurjchem-1596	193	23	.	.	PUNCT
eurjchem-1596	194	1	264	264	NUM
eurjchem-1596	194	2	pappula	pappula	NOUN
eurjchem-1596	194	3	et	et	PROPN
eurjchem-1596	194	4	al	al	PROPN
eurjchem-1596	194	5	.	.	PUNCT
eurjchem-1596	194	6	/	/	SYM
eurjchem-1596	194	7	european	european	PROPN
eurjchem-1596	194	8	journal	journal	PROPN
eurjchem-1596	194	9	of	of	ADP
eurjchem-1596	194	10	chemistry	chemistry	NOUN
eurjchem-1596	194	11	8	8	NUM
eurjchem-1596	194	12	(	(	PUNCT
eurjchem-1596	194	13	3	3	NUM
eurjchem-1596	194	14	)	)	PUNCT
eurjchem-1596	194	15	(	(	PUNCT
eurjchem-1596	194	16	2017	2017	NUM
eurjchem-1596	194	17	)	)	PUNCT
eurjchem-1596	194	18	258‐264	258‐264	NUM
eurjchem-1596	194	19	figure	figure	NOUN
eurjchem-1596	194	20	6	6	NUM
eurjchem-1596	194	21	.	.	PUNCT
eurjchem-1596	194	22	istd	istd	NOUN
eurjchem-1596	194	23	trend	trend	NOUN
eurjchem-1596	194	24	in	in	ADP
eurjchem-1596	194	25	extended	extended	ADJ
eurjchem-1596	194	26	run	run	NOUN
eurjchem-1596	194	27	accuracy	accuracy	NOUN
eurjchem-1596	194	28	.	.	PUNCT
eurjchem-1596	195	1	the	the	DET
eurjchem-1596	195	2	unknown	unknown	ADJ
eurjchem-1596	195	3	sample	sample	NOUN
eurjchem-1596	195	4	istd	istd	NOUN
eurjchem-1596	195	5	response	response	NOUN
eurjchem-1596	195	6	should	should	AUX
eurjchem-1596	195	7	be	be	AUX
eurjchem-1596	195	8	within	within	ADP
eurjchem-1596	195	9	50‐	50‐	NUM
eurjchem-1596	195	10	150	150	NUM
eurjchem-1596	195	11	%	%	NOUN
eurjchem-1596	195	12	of	of	ADP
eurjchem-1596	195	13	average	average	ADJ
eurjchem-1596	195	14	response	response	NOUN
eurjchem-1596	195	15	.	.	PUNCT
eurjchem-1596	196	1	the	the	DET
eurjchem-1596	196	2	slow	slow	ADJ
eurjchem-1596	196	3	fall	fall	NOUN
eurjchem-1596	196	4	or	or	CCONJ
eurjchem-1596	196	5	raise	raise	VERB
eurjchem-1596	196	6	in	in	ADP
eurjchem-1596	196	7	response	response	NOUN
eurjchem-1596	196	8	of	of	ADP
eurjchem-1596	196	9	istd	istd	NOUN
eurjchem-1596	196	10	was	be	AUX
eurjchem-1596	196	11	not	not	PART
eurjchem-1596	196	12	considered	consider	VERB
eurjchem-1596	196	13	and	and	CCONJ
eurjchem-1596	196	14	addressed	address	VERB
eurjchem-1596	196	15	in	in	ADP
eurjchem-1596	196	16	the	the	DET
eurjchem-1596	196	17	above	above	ADJ
eurjchem-1596	196	18	format	format	NOUN
eurjchem-1596	196	19	but	but	CCONJ
eurjchem-1596	196	20	it	it	PRON
eurjchem-1596	196	21	will	will	AUX
eurjchem-1596	196	22	affect	affect	VERB
eurjchem-1596	196	23	the	the	DET
eurjchem-1596	196	24	unknown	unknown	ADJ
eurjchem-1596	196	25	sample	sample	NOUN
eurjchem-1596	196	26	concentration	concentration	NOUN
eurjchem-1596	196	27	by	by	ADP
eurjchem-1596	196	28	more	more	ADJ
eurjchem-1596	196	29	than	than	ADP
eurjchem-1596	196	30	15	15	NUM
eurjchem-1596	196	31	%	%	NOUN
eurjchem-1596	196	32	.	.	PUNCT
eurjchem-1596	197	1	to	to	PART
eurjchem-1596	197	2	know	know	VERB
eurjchem-1596	197	3	istd	istd	NOUN
eurjchem-1596	197	4	response	response	NOUN
eurjchem-1596	197	5	trend	trend	NOUN
eurjchem-1596	197	6	in	in	ADP
eurjchem-1596	197	7	overall	overall	ADJ
eurjchem-1596	197	8	analytical	analytical	ADJ
eurjchem-1596	197	9	run	run	NOUN
eurjchem-1596	197	10	,	,	PUNCT
eurjchem-1596	197	11	the	the	DET
eurjchem-1596	197	12	absolute	absolute	ADJ
eurjchem-1596	197	13	deviation	deviation	NOUN
eurjchem-1596	197	14	between	between	ADP
eurjchem-1596	197	15	the	the	DET
eurjchem-1596	197	16	average	average	ADJ
eurjchem-1596	197	17	areas	area	NOUN
eurjchem-1596	197	18	analyte	analyte	NOUN
eurjchem-1596	197	19	and	and	CCONJ
eurjchem-1596	197	20	istd	istd	NOUN
eurjchem-1596	197	21	were	be	AUX
eurjchem-1596	197	22	calculated	calculate	VERB
eurjchem-1596	197	23	and	and	CCONJ
eurjchem-1596	197	24	the	the	DET
eurjchem-1596	197	25	deviation	deviation	NOUN
eurjchem-1596	197	26	is	be	AUX
eurjchem-1596	197	27	3.6	3.6	NUM
eurjchem-1596	197	28	%	%	NOUN
eurjchem-1596	197	29	.	.	PUNCT
eurjchem-1596	198	1	the	the	DET
eurjchem-1596	198	2	overall	overall	ADJ
eurjchem-1596	198	3	precision	precision	NOUN
eurjchem-1596	198	4	for	for	ADP
eurjchem-1596	198	5	istd	istd	NOUN
eurjchem-1596	198	6	response	response	NOUN
eurjchem-1596	198	7	is	be	AUX
eurjchem-1596	198	8	5.1	5.1	NUM
eurjchem-1596	198	9	%	%	NOUN
eurjchem-1596	198	10	.	.	PUNCT
eurjchem-1596	199	1	the	the	DET
eurjchem-1596	199	2	result	result	NOUN
eurjchem-1596	199	3	of	of	ADP
eurjchem-1596	199	4	istd	istd	NOUN
eurjchem-1596	199	5	trend	trend	NOUN
eurjchem-1596	199	6	analysis	analysis	NOUN
eurjchem-1596	199	7	proves	prove	VERB
eurjchem-1596	199	8	method	method	NOUN
eurjchem-1596	199	9	diversity	diversity	NOUN
eurjchem-1596	199	10	and	and	CCONJ
eurjchem-1596	199	11	reproducibility	reproducibility	NOUN
eurjchem-1596	199	12	.	.	PUNCT
eurjchem-1596	200	1	the	the	DET
eurjchem-1596	200	2	istd	istd	NOUN
eurjchem-1596	200	3	trend	trend	NOUN
eurjchem-1596	200	4	in	in	ADP
eurjchem-1596	200	5	extended	extended	ADJ
eurjchem-1596	200	6	run	run	NOUN
eurjchem-1596	200	7	accuracy	accuracy	NOUN
eurjchem-1596	200	8	was	be	AUX
eurjchem-1596	200	9	shown	show	VERB
eurjchem-1596	200	10	in	in	ADP
eurjchem-1596	200	11	figure	figure	NOUN
eurjchem-1596	200	12	6	6	NUM
eurjchem-1596	200	13	.	.	NOUN
eurjchem-1596	200	14	4	4	NUM
eurjchem-1596	200	15	.	.	X
eurjchem-1596	200	16	conclusion	conclusion	NOUN
eurjchem-1596	200	17	for	for	ADP
eurjchem-1596	200	18	monitoring	monitor	VERB
eurjchem-1596	200	19	ulipristal	ulipristal	ADJ
eurjchem-1596	200	20	acetate	acetate	NOUN
eurjchem-1596	200	21	concentration	concentration	NOUN
eurjchem-1596	200	22	in	in	ADP
eurjchem-1596	200	23	human	human	ADJ
eurjchem-1596	200	24	plasma	plasma	NOUN
eurjchem-1596	200	25	,	,	PUNCT
eurjchem-1596	200	26	a	a	DET
eurjchem-1596	200	27	specific	specific	ADJ
eurjchem-1596	200	28	,	,	PUNCT
eurjchem-1596	200	29	selective	selective	ADJ
eurjchem-1596	200	30	,	,	PUNCT
eurjchem-1596	200	31	fast	fast	ADJ
eurjchem-1596	200	32	,	,	PUNCT
eurjchem-1596	200	33	sensitive	sensitive	ADJ
eurjchem-1596	200	34	and	and	CCONJ
eurjchem-1596	200	35	accurate	accurate	ADJ
eurjchem-1596	200	36	lc‐	lc‐	ADJ
eurjchem-1596	200	37	ms	ms	PROPN
eurjchem-1596	200	38	/	/	SYM
eurjchem-1596	200	39	ms	ms	PROPN
eurjchem-1596	200	40	method	method	NOUN
eurjchem-1596	200	41	was	be	AUX
eurjchem-1596	200	42	developed	develop	VERB
eurjchem-1596	200	43	and	and	CCONJ
eurjchem-1596	200	44	fully	fully	ADV
eurjchem-1596	200	45	validated	validate	VERB
eurjchem-1596	200	46	in	in	ADP
eurjchem-1596	200	47	the	the	DET
eurjchem-1596	200	48	range	range	NOUN
eurjchem-1596	200	49	of	of	ADP
eurjchem-1596	200	50	1‐300	1‐300	NUM
eurjchem-1596	200	51	ng	ng	PROPN
eurjchem-1596	200	52	/	/	SYM
eurjchem-1596	200	53	ml	ml	PROPN
eurjchem-1596	200	54	.	.	PUNCT
eurjchem-1596	201	1	the	the	DET
eurjchem-1596	201	2	validation	validation	NOUN
eurjchem-1596	201	3	result	result	NOUN
eurjchem-1596	201	4	shows	show	VERB
eurjchem-1596	201	5	that	that	SCONJ
eurjchem-1596	201	6	the	the	DET
eurjchem-1596	201	7	method	method	NOUN
eurjchem-1596	201	8	is	be	AUX
eurjchem-1596	201	9	repeatable	repeatable	ADJ
eurjchem-1596	201	10	,	,	PUNCT
eurjchem-1596	201	11	reproducible	reproducible	ADJ
eurjchem-1596	201	12	and	and	CCONJ
eurjchem-1596	201	13	robust	robust	ADJ
eurjchem-1596	201	14	.	.	PUNCT
eurjchem-1596	202	1	it	it	PRON
eurjchem-1596	202	2	can	can	AUX
eurjchem-1596	202	3	be	be	AUX
eurjchem-1596	202	4	applied	apply	VERB
eurjchem-1596	202	5	for	for	ADP
eurjchem-1596	202	6	bioequivalence	bioequivalence	NOUN
eurjchem-1596	202	7	studies	study	NOUN
eurjchem-1596	202	8	and	and	CCONJ
eurjchem-1596	202	9	larger	large	ADJ
eurjchem-1596	202	10	pharmacokinetic	pharmacokinetic	ADJ
eurjchem-1596	202	11	thera‐	thera‐	PRON
eurjchem-1596	202	12	peutic	peutic	ADJ
eurjchem-1596	202	13	monitoring	monitoring	NOUN
eurjchem-1596	202	14	studies	study	NOUN
eurjchem-1596	202	15	in	in	ADP
eurjchem-1596	202	16	patients	patient	NOUN
eurjchem-1596	202	17	and	and	CCONJ
eurjchem-1596	202	18	in	in	ADP
eurjchem-1596	202	19	healthy	healthy	ADJ
eurjchem-1596	202	20	volun‐	volun‐	NOUN
eurjchem-1596	202	21	teers	teer	NOUN
eurjchem-1596	202	22	.	.	PUNCT
eurjchem-1596	203	1	acknowledgements	acknowledgement	NOUN
eurjchem-1596	203	2	the	the	DET
eurjchem-1596	203	3	authors	author	NOUN
eurjchem-1596	203	4	are	be	AUX
eurjchem-1596	203	5	wishing	wish	VERB
eurjchem-1596	203	6	to	to	PART
eurjchem-1596	203	7	acknowledge	acknowledge	VERB
eurjchem-1596	203	8	staff	staff	NOUN
eurjchem-1596	203	9	members	member	NOUN
eurjchem-1596	203	10	for	for	ADP
eurjchem-1596	203	11	useful	useful	ADJ
eurjchem-1596	203	12	and	and	CCONJ
eurjchem-1596	203	13	valuable	valuable	ADJ
eurjchem-1596	203	14	discussions	discussion	NOUN
eurjchem-1596	203	15	references	reference	NOUN
eurjchem-1596	203	16	[	[	X
eurjchem-1596	203	17	1	1	NUM
eurjchem-1596	203	18	]	]	PUNCT
eurjchem-1596	203	19	.	.	PUNCT
eurjchem-1596	204	1	gemzell‐danielsson	gemzell‐danielsson	PROPN
eurjchem-1596	204	2	,	,	PUNCT
eurjchem-1596	204	3	k.	k.	PROPN
eurjchem-1596	204	4	;	;	PUNCT
eurjchem-1596	204	5	chun‐xia	chun‐xia	NOUN
eurjchem-1596	204	6	,	,	PUNCT
eurjchem-1596	204	7	m.	m.	NOUN
eurjchem-1596	204	8	int	int	PROPN
eurjchem-1596	204	9	.	.	PUNCT
eurjchem-1596	205	1	j.	j.	PROPN
eurjchem-1596	205	2	womens	womens	PROPN
eurjchem-1596	205	3	health	health	PROPN
eurjchem-1596	205	4	.	.	PUNCT
eurjchem-1596	206	1	2010	2010	NUM
eurjchem-1596	206	2	,	,	PUNCT
eurjchem-1596	206	3	2	2	NUM
eurjchem-1596	206	4	,	,	PUNCT
eurjchem-1596	206	5	53‐61	53‐61	NUM
eurjchem-1596	206	6	.	.	PUNCT
eurjchem-1596	207	1	[	[	X
eurjchem-1596	207	2	2	2	NUM
eurjchem-1596	207	3	]	]	PUNCT
eurjchem-1596	207	4	.	.	PUNCT
eurjchem-1596	208	1	goldstajn	goldstajn	PROPN
eurjchem-1596	208	2	,	,	PUNCT
eurjchem-1596	208	3	m.	m.	NOUN
eurjchem-1596	208	4	s.	s.	PROPN
eurjchem-1596	208	5	;	;	PUNCT
eurjchem-1596	208	6	baldani	baldani	PROPN
eurjchem-1596	208	7	,	,	PUNCT
eurjchem-1596	208	8	d.	d.	PROPN
eurjchem-1596	208	9	p.	p.	PROPN
eurjchem-1596	208	10	;	;	PUNCT
eurjchem-1596	209	1	škrgatić	škrgatić	PROPN
eurjchem-1596	209	2	,	,	PUNCT
eurjchem-1596	209	3	l.	l.	PROPN
eurjchem-1596	209	4	;	;	PUNCT
eurjchem-1596	209	5	radaković	radaković	PROPN
eurjchem-1596	209	6	,	,	PUNCT
eurjchem-1596	209	7	b.	b.	PROPN
eurjchem-1596	209	8	;	;	PUNCT
eurjchem-1596	209	9	vrčić	vrčić	PROPN
eurjchem-1596	209	10	,	,	PUNCT
eurjchem-1596	209	11	h.	h.	PROPN
eurjchem-1596	209	12	;	;	PUNCT
eurjchem-1596	209	13	čanić	čanić	NOUN
eurjchem-1596	209	14	,	,	PUNCT
eurjchem-1596	209	15	t.	t.	NOUN
eurjchem-1596	209	16	collegium	collegium	NOUN
eurjchem-1596	209	17	antropol	antropol	NOUN
eurjchem-1596	209	18	.	.	PUNCT
eurjchem-1596	210	1	2014	2014	NUM
eurjchem-1596	210	2	,	,	PUNCT
eurjchem-1596	210	3	38	38	NUM
eurjchem-1596	210	4	,	,	PUNCT
eurjchem-1596	210	5	379‐384	379‐384	NUM
eurjchem-1596	210	6	.	.	PUNCT
eurjchem-1596	211	1	[	[	X
eurjchem-1596	211	2	3	3	NUM
eurjchem-1596	211	3	]	]	PUNCT
eurjchem-1596	211	4	.	.	PUNCT
eurjchem-1596	212	1	richardson	richardson	PROPN
eurjchem-1596	212	2	,	,	PUNCT
eurjchem-1596	212	3	a.	a.	PROPN
eurjchem-1596	212	4	r.	r.	PROPN
eurjchem-1596	212	5	;	;	PUNCT
eurjchem-1596	212	6	fraidy	fraidy	ADJ
eurjchem-1596	212	7	,	,	PUNCT
eurjchem-1596	212	8	n.	n.	PROPN
eurjchem-1596	212	9	clin	clin	PROPN
eurjchem-1596	212	10	.	.	PUNCT
eurjchem-1596	213	1	ther	ther	PROPN
eurjchem-1596	213	2	.	.	PUNCT
eurjchem-1596	214	1	2012	2012	NUM
eurjchem-1596	214	2	,	,	PUNCT
eurjchem-1596	214	3	1	1	NUM
eurjchem-1596	214	4	,	,	PUNCT
eurjchem-1596	214	5	24‐36	24‐36	NUM
eurjchem-1596	214	6	.	.	PUNCT
eurjchem-1596	215	1	[	[	X
eurjchem-1596	215	2	4	4	NUM
eurjchem-1596	215	3	]	]	PUNCT
eurjchem-1596	215	4	.	.	PUNCT
eurjchem-1596	215	5	brache	brache	PROPN
eurjchem-1596	215	6	,	,	PUNCT
eurjchem-1596	215	7	v.	v.	PROPN
eurjchem-1596	215	8	;	;	PUNCT
eurjchem-1596	215	9	cochon	cochon	PROPN
eurjchem-1596	215	10	,	,	PUNCT
eurjchem-1596	215	11	l.	l.	PROPN
eurjchem-1596	215	12	;	;	PUNCT
eurjchem-1596	215	13	jesam	jesam	PROPN
eurjchem-1596	215	14	,	,	PUNCT
eurjchem-1596	215	15	c.	c.	PROPN
eurjchem-1596	215	16	;	;	PUNCT
eurjchem-1596	215	17	maldonado	maldonado	PROPN
eurjchem-1596	215	18	,	,	PUNCT
eurjchem-1596	215	19	r.	r.	PROPN
eurjchem-1596	215	20	;	;	PUNCT
eurjchem-1596	215	21	salvatierra	salvatierra	PROPN
eurjchem-1596	215	22	,	,	PUNCT
eurjchem-1596	215	23	a.	a.	NOUN
eurjchem-1596	215	24	m.	m.	NOUN
eurjchem-1596	215	25	;	;	PUNCT
eurjchem-1596	215	26	levy	levy	NOUN
eurjchem-1596	215	27	,	,	PUNCT
eurjchem-1596	215	28	d.	d.	PROPN
eurjchem-1596	215	29	p.	p.	PROPN
eurjchem-1596	215	30	;	;	PUNCT
eurjchem-1596	215	31	gainer	gainer	PROPN
eurjchem-1596	215	32	,	,	PUNCT
eurjchem-1596	215	33	e.	e.	PROPN
eurjchem-1596	215	34	;	;	PUNCT
eurjchem-1596	215	35	croxatto	croxatto	PROPN
eurjchem-1596	215	36	,	,	PUNCT
eurjchem-1596	215	37	h.	h.	PROPN
eurjchem-1596	215	38	b.	b.	PROPN
eurjchem-1596	215	39	hum	hum	PROPN
eurjchem-1596	215	40	.	.	PUNCT
eurjchem-1596	216	1	reprod	reprod	PROPN
eurjchem-1596	216	2	.	.	PUNCT
eurjchem-1596	217	1	2010	2010	NUM
eurjchem-1596	217	2	,	,	PUNCT
eurjchem-1596	217	3	25	25	NUM
eurjchem-1596	217	4	,	,	PUNCT
eurjchem-1596	217	5	2256‐	2256‐	NUM
eurjchem-1596	217	6	2263	2263	NUM
eurjchem-1596	217	7	.	.	PUNCT
eurjchem-1596	218	1	[	[	X
eurjchem-1596	218	2	5	5	NUM
eurjchem-1596	218	3	]	]	PUNCT
eurjchem-1596	218	4	.	.	PUNCT
eurjchem-1596	219	1	pohl	pohl	PROPN
eurjchem-1596	219	2	,	,	PUNCT
eurjchem-1596	219	3	o.	o.	PROPN
eurjchem-1596	219	4	;	;	PUNCT
eurjchem-1596	219	5	zobrist	zobrist	PROPN
eurjchem-1596	219	6	,	,	PUNCT
eurjchem-1596	219	7	r.	r.	PROPN
eurjchem-1596	219	8	h.	h.	PROPN
eurjchem-1596	219	9	;	;	PUNCT
eurjchem-1596	219	10	gotteland	gotteland	PROPN
eurjchem-1596	219	11	,	,	PUNCT
eurjchem-1596	219	12	j.	j.	PROPN
eurjchem-1596	219	13	p.	p.	PROPN
eurjchem-1596	219	14	reprod	reprod	PROPN
eurjchem-1596	219	15	.	.	PUNCT
eurjchem-1596	220	1	sci	sci	PROPN
eurjchem-1596	220	2	.	.	PROPN
eurjchem-1596	220	3	2015	2015	NUM
eurjchem-1596	220	4	,	,	PUNCT
eurjchem-1596	220	5	22	22	NUM
eurjchem-1596	220	6	,	,	PUNCT
eurjchem-1596	220	7	476‐483	476‐483	NUM
eurjchem-1596	220	8	.	.	PUNCT
eurjchem-1596	221	1	[	[	X
eurjchem-1596	221	2	6	6	NUM
eurjchem-1596	221	3	]	]	PUNCT
eurjchem-1596	221	4	.	.	PUNCT
eurjchem-1596	222	1	jadav	jadav	PROPN
eurjchem-1596	222	2	,	,	PUNCT
eurjchem-1596	222	3	s.	s.	PROPN
eurjchem-1596	222	4	p.	p.	PROPN
eurjchem-1596	222	5	;	;	PUNCT
eurjchem-1596	223	1	parmar	parmar	PROPN
eurjchem-1596	223	2	,	,	PUNCT
eurjchem-1596	223	3	d.	d.	PROPN
eurjchem-1596	223	4	m.	m.	PROPN
eurjchem-1596	223	5	j.	j.	PROPN
eurjchem-1596	223	6	pharmacol	pharmacol	PROPN
eurjchem-1596	223	7	.	.	PUNCT
eurjchem-1596	224	1	pharmacother	pharmacother	PROPN
eurjchem-1596	224	2	.	.	PUNCT
eurjchem-1596	225	1	2012	2012	NUM
eurjchem-1596	225	2	,	,	PUNCT
eurjchem-1596	225	3	3(2	3(2	NUM
eurjchem-1596	225	4	)	)	PUNCT
eurjchem-1596	225	5	,	,	PUNCT
eurjchem-1596	225	6	109‐111	109‐111	NUM
eurjchem-1596	225	7	.	.	PUNCT
eurjchem-1596	226	1	[	[	X
eurjchem-1596	226	2	7	7	NUM
eurjchem-1596	226	3	]	]	PUNCT
eurjchem-1596	226	4	.	.	PUNCT
eurjchem-1596	227	1	shi	shi	PROPN
eurjchem-1596	227	2	,	,	PUNCT
eurjchem-1596	227	3	j.	j.	PROPN
eurjchem-1596	227	4	x.	x.	PROPN
eurjchem-1596	227	5	;	;	PUNCT
eurjchem-1596	227	6	zhu	zhu	PROPN
eurjchem-1596	227	7	,	,	PUNCT
eurjchem-1596	227	8	f.	f.	PROPN
eurjchem-1596	227	9	y.	y.	PROPN
eurjchem-1596	227	10	;	;	PUNCT
eurjchem-1596	227	11	zou	zou	PROPN
eurjchem-1596	227	12	,	,	PUNCT
eurjchem-1596	227	13	q.	q.	PROPN
eurjchem-1596	227	14	g.	g.	PROPN
eurjchem-1596	227	15	;	;	PUNCT
eurjchem-1596	227	16	sun	sun	PROPN
eurjchem-1596	227	17	,	,	PUNCT
eurjchem-1596	227	18	l.	l.	PROPN
eurjchem-1596	227	19	l	l	PROPN
eurjchem-1596	227	20	;	;	PUNCT
eurjchem-1596	227	21	wei	wei	PROPN
eurjchem-1596	227	22	,	,	PUNCT
eurjchem-1596	227	23	p.	p.	NOUN
eurjchem-1596	227	24	chin	chin	PROPN
eurjchem-1596	227	25	.	.	PUNCT
eurjchem-1596	228	1	j.	j.	PROPN
eurjchem-1596	228	2	new	new	ADJ
eurjchem-1596	228	3	drugs	drug	NOUN
eurjchem-1596	228	4	2014	2014	NUM
eurjchem-1596	228	5	,	,	PUNCT
eurjchem-1596	228	6	7	7	NUM
eurjchem-1596	228	7	,	,	PUNCT
eurjchem-1596	228	8	839‐852	839‐852	NUM
eurjchem-1596	228	9	.	.	PUNCT
eurjchem-1596	229	1	[	[	X
eurjchem-1596	229	2	8	8	NUM
eurjchem-1596	229	3	]	]	PUNCT
eurjchem-1596	229	4	.	.	PUNCT
eurjchem-1596	230	1	pohl	pohl	PROPN
eurjchem-1596	230	2	,	,	PUNCT
eurjchem-1596	230	3	o.	o.	PROPN
eurjchem-1596	230	4	;	;	PUNCT
eurjchem-1596	230	5	williams	williams	PROPN
eurjchem-1596	230	6	,	,	PUNCT
eurjchem-1596	230	7	a.	a.	PROPN
eurjchem-1596	230	8	r.	r.	PROPN
eurjchem-1596	230	9	;	;	PUNCT
eurjchem-1596	230	10	bergeron	bergeron	PROPN
eurjchem-1596	230	11	,	,	PUNCT
eurjchem-1596	230	12	c.	c.	PROPN
eurjchem-1596	230	13	b.	b.	PROPN
eurjchem-1596	230	14	;	;	PUNCT
eurjchem-1596	230	15	gotteland	gotteland	PROPN
eurjchem-1596	230	16	,	,	PUNCT
eurjchem-1596	230	17	j.	j.	PROPN
eurjchem-1596	230	18	p.	p.	PROPN
eurjchem-1596	230	19	regul	regul	PROPN
eurjchem-1596	230	20	.	.	PUNCT
eurjchem-1596	231	1	toxicol	toxicol	PROPN
eurjchem-1596	231	2	.	.	PUNCT
eurjchem-1596	232	1	pharmacol	pharmacol	PROPN
eurjchem-1596	232	2	.	.	PUNCT
eurjchem-1596	233	1	2013	2013	NUM
eurjchem-1596	233	2	,	,	PUNCT
eurjchem-1596	233	3	66	66	NUM
eurjchem-1596	233	4	,	,	PUNCT
eurjchem-1596	233	5	6‐12	6‐12	NUM
eurjchem-1596	233	6	.	.	PUNCT
eurjchem-1596	234	1	[	[	X
eurjchem-1596	234	2	9	9	NUM
eurjchem-1596	234	3	]	]	PUNCT
eurjchem-1596	234	4	.	.	PUNCT
eurjchem-1596	235	1	guidance	guidance	NOUN
eurjchem-1596	235	2	for	for	ADP
eurjchem-1596	235	3	industry	industry	NOUN
eurjchem-1596	235	4	:	:	PUNCT
eurjchem-1596	235	5	bioanalytical	bioanalytical	ADJ
eurjchem-1596	235	6	method	method	NOUN
eurjchem-1596	235	7	validation	validation	NOUN
eurjchem-1596	235	8	,	,	PUNCT
eurjchem-1596	235	9	u.	u.	PROPN
eurjchem-1596	235	10	s.	s.	PROPN
eurjchem-1596	235	11	department	department	PROPN
eurjchem-1596	235	12	of	of	ADP
eurjchem-1596	235	13	health	health	PROPN
eurjchem-1596	235	14	and	and	CCONJ
eurjchem-1596	235	15	human	human	ADJ
eurjchem-1596	235	16	services	service	NOUN
eurjchem-1596	235	17	,	,	PUNCT
eurjchem-1596	235	18	food	food	NOUN
eurjchem-1596	235	19	and	and	CCONJ
eurjchem-1596	235	20	drug	drug	NOUN
eurjchem-1596	235	21	administration	administration	NOUN
eurjchem-1596	235	22	,	,	PUNCT
eurjchem-1596	235	23	may	may	AUX
eurjchem-1596	235	24	2001	2001	NUM
eurjchem-1596	235	25	,	,	PUNCT
eurjchem-1596	235	26	rockville	rockville	PROPN
eurjchem-1596	235	27	,	,	PUNCT
eurjchem-1596	235	28	md	md	PROPN
eurjchem-1596	235	29	,	,	PUNCT
eurjchem-1596	235	30	usa	usa	PROPN
eurjchem-1596	235	31	.	.	PUNCT
eurjchem-1596	236	1	[	[	X
eurjchem-1596	236	2	10	10	NUM
eurjchem-1596	236	3	]	]	PUNCT
eurjchem-1596	236	4	.	.	PUNCT
eurjchem-1596	237	1	bioanalytical	bioanalytical	ADJ
eurjchem-1596	237	2	method	method	PROPN
eurjchem-1596	237	3	validation	validation	NOUN
eurjchem-1596	237	4	guideline	guideline	NOUN
eurjchem-1596	237	5	,	,	PUNCT
eurjchem-1596	237	6	brazil	brazil	PROPN
eurjchem-1596	237	7	,	,	PUNCT
eurjchem-1596	237	8	agenda	agenda	PROPN
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eurjchem-1596	237	10	sanitaria	sanitaria	PROPN
eurjchem-1596	237	11	(	(	PUNCT
eurjchem-1596	237	12	anvisa	anvisa	NOUN
eurjchem-1596	237	13	)	)	PUNCT
eurjchem-1596	237	14	resolution‐rdc	resolution‐rdc	NOUN
eurjchem-1596	238	1	no	no	INTJ
eurjchem-1596	238	2	.	.	PROPN
eurjchem-1596	238	3	27	27	NUM
eurjchem-1596	238	4	,	,	PUNCT
eurjchem-1596	238	5	may	may	AUX
eurjchem-1596	238	6	17	17	NUM
eurjchem-1596	238	7	,	,	PUNCT
eurjchem-1596	238	8	2012	2012	NUM
eurjchem-1596	238	9	.	.	PUNCT
eurjchem-1596	239	1	[	[	X
eurjchem-1596	239	2	11	11	NUM
eurjchem-1596	239	3	]	]	PUNCT
eurjchem-1596	239	4	.	.	PUNCT
eurjchem-1596	240	1	ye	ye	PROPN
eurjchem-1596	240	2	,	,	PUNCT
eurjchem-1596	240	3	j.	j.	PROPN
eurjchem-1596	240	4	h.	h.	PROPN
eurjchem-1596	240	5	;	;	PUNCT
eurjchem-1596	240	6	pao	pao	PROPN
eurjchem-1596	240	7	,	,	PUNCT
eurjchem-1596	240	8	l.	l.	PROPN
eurjchem-1596	240	9	h.	h.	PROPN
eurjchem-1596	240	10	plos	plos	PROPN
eurjchem-1596	240	11	one	one	NUM
eurjchem-1596	240	12	2014	2014	NUM
eurjchem-1596	240	13	,	,	PUNCT
eurjchem-1596	240	14	24	24	NUM
eurjchem-1596	240	15	,	,	PUNCT
eurjchem-1596	240	16	1‐18	1‐18	NUM
eurjchem-1596	240	17	.	.	PUNCT
eurjchem-1596	241	1	[	[	X
eurjchem-1596	241	2	12	12	NUM
eurjchem-1596	241	3	]	]	PUNCT
eurjchem-1596	241	4	.	.	PUNCT
eurjchem-1596	242	1	ismaiel	ismaiel	ADJ
eurjchem-1596	242	2	,	,	PUNCT
eurjchem-1596	242	3	o.	o.	NOUN
eurjchem-1596	242	4	a.	a.	NOUN
eurjchem-1596	242	5	;	;	PUNCT
eurjchem-1596	242	6	halquist	halquist	NOUN
eurjchem-1596	242	7	,	,	PUNCT
eurjchem-1596	242	8	m.	m.	NOUN
eurjchem-1596	242	9	s.	s.	PROPN
eurjchem-1596	242	10	;	;	PUNCT
eurjchem-1596	242	11	elmamly	elmamly	ADV
eurjchem-1596	242	12	,	,	PUNCT
eurjchem-1596	242	13	m.	m.	NOUN
eurjchem-1596	242	14	y.	y.	PROPN
eurjchem-1596	242	15	;	;	PUNCT
eurjchem-1596	242	16	shalaby	shalaby	PROPN
eurjchem-1596	242	17	,	,	PUNCT
eurjchem-1596	242	18	a.	a.	NOUN
eurjchem-1596	242	19	;	;	PUNCT
eurjchem-1596	242	20	karnes	karnes	PROPN
eurjchem-1596	242	21	,	,	PUNCT
eurjchem-1596	242	22	h.	h.	PROPN
eurjchem-1596	242	23	t.	t.	PROPN
eurjchem-1596	242	24	j.	j.	PROPN
eurjchem-1596	242	25	chromatogr	chromatogr	PROPN
eurjchem-1596	242	26	.	.	PUNCT
eurjchem-1596	243	1	b	b	X
eurjchem-1596	243	2	:	:	PUNCT
eurjchem-1596	243	3	anal	anal	ADJ
eurjchem-1596	243	4	.	.	PUNCT
eurjchem-1596	244	1	technol	technol	PROPN
eurjchem-1596	244	2	.	.	PROPN
eurjchem-1596	244	3	biomed	biome	VERB
eurjchem-1596	244	4	.	.	PUNCT
eurjchem-1596	245	1	life	life	PROPN
eurjchem-1596	245	2	sci	sci	PROPN
eurjchem-1596	245	3	.	.	PROPN
eurjchem-1596	245	4	2007	2007	NUM
eurjchem-1596	245	5	,	,	PUNCT
eurjchem-1596	245	6	859	859	NUM
eurjchem-1596	245	7	,	,	PUNCT
eurjchem-1596	245	8	84‐93	84‐93	NUM
eurjchem-1596	245	9	.	.	PUNCT
eurjchem-1596	246	1	[	[	X
eurjchem-1596	246	2	13	13	NUM
eurjchem-1596	246	3	]	]	PUNCT
eurjchem-1596	246	4	.	.	PUNCT
eurjchem-1596	247	1	www.medicines.org.uk/emc/medicine/26068/spc/#pharmacoki	www.medicines.org.uk/emc/medicine/26068/spc/#pharmacoki	PROPN
eurjchem-1596	247	2	netic_props	netic_prop	NOUN
eurjchem-1596	247	3	viewed	view	VERB
eurjchem-1596	247	4	05	05	NUM
eurjchem-1596	247	5	august	august	PROPN
eurjchem-1596	247	6	2017	2017	NUM
eurjchem-1596	247	7	.	.	PUNCT