id	sid	tid	token	lemma	pos
eurjchem-1602	1	1	untitled	untitle	VERB
eurjchem-1602	1	2	european	european	PROPN
eurjchem-1602	1	3	journal	journal	PROPN
eurjchem-1602	1	4	of	of	ADP
eurjchem-1602	1	5	chemistry	chemistry	NOUN
eurjchem-1602	1	6	8	8	NUM
eurjchem-1602	1	7	(	(	PUNCT
eurjchem-1602	1	8	3	3	NUM
eurjchem-1602	1	9	)	)	PUNCT
eurjchem-1602	1	10	(	(	PUNCT
eurjchem-1602	1	11	2017	2017	NUM
eurjchem-1602	1	12	)	)	PUNCT
eurjchem-1602	1	13	248‐251	248‐251	PROPN
eurjchem-1602	1	14	european	european	PROPN
eurjchem-1602	1	15	journal	journal	PROPN
eurjchem-1602	1	16	of	of	ADP
eurjchem-1602	1	17	chemistry	chemistry	NOUN
eurjchem-1602	1	18	issn	issn	PROPN
eurjchem-1602	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-1602	1	20	(	(	PUNCT
eurjchem-1602	1	21	print	print	NOUN
eurjchem-1602	1	22	)	)	PUNCT
eurjchem-1602	1	23	/	/	SYM
eurjchem-1602	1	24	issn	issn	PROPN
eurjchem-1602	1	25	2153‐2257	2153‐2257	NUM
eurjchem-1602	1	26	(	(	PUNCT
eurjchem-1602	1	27	online	online	ADJ
eurjchem-1602	1	28	)	)	PUNCT
eurjchem-1602	1	29			NOUN
eurjchem-1602	1	30	2017	2017	NUM
eurjchem-1602	1	31	atlanta	atlanta	PROPN
eurjchem-1602	1	32	publishing	publishing	PROPN
eurjchem-1602	1	33	house	house	PROPN
eurjchem-1602	1	34	llc	llc	PROPN
eurjchem-1602	1	35	‐	‐	PUNCT
eurjchem-1602	1	36	all	all	DET
eurjchem-1602	1	37	rights	right	NOUN
eurjchem-1602	1	38	reserved	reserve	VERB
eurjchem-1602	1	39	‐	‐	NOUN
eurjchem-1602	1	40	printed	print	VERB
eurjchem-1602	1	41	in	in	ADP
eurjchem-1602	1	42	the	the	DET
eurjchem-1602	1	43	usa	usa	PROPN
eurjchem-1602	1	44	http://dx.doi.org/10.5155/eurjchem.8.3.248-251.1602	http://dx.doi.org/10.5155/eurjchem.8.3.248-251.1602	PROPN
eurjchem-1602	1	45	european	european	PROPN
eurjchem-1602	1	46	journal	journal	PROPN
eurjchem-1602	1	47	of	of	ADP
eurjchem-1602	1	48	chemistry	chemistry	PROPN
eurjchem-1602	1	49	journal	journal	PROPN
eurjchem-1602	1	50	webpage	webpage	NOUN
eurjchem-1602	1	51	:	:	PUNCT
eurjchem-1602	2	1	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1602	2	2	synthesis	synthesis	NOUN
eurjchem-1602	2	3	and	and	CCONJ
eurjchem-1602	2	4	x‐ray	x‐ray	ADJ
eurjchem-1602	2	5	crystallography	crystallography	NOUN
eurjchem-1602	2	6	of	of	ADP
eurjchem-1602	2	7	(	(	PUNCT
eurjchem-1602	2	8	1r,3ar,7ar)‐1‐((s)‐1‐((2r,5s)‐5‐(3‐	1r,3ar,7ar)‐1‐((s)‐1‐((2r,5s)‐5‐(3‐	PROPN
eurjchem-1602	2	9	hydroxypentan‐3‐yl)tetrahydrofuran‐2‐yl)ethyl)‐7a‐methyloctahydro‐4h‐	hydroxypentan‐3‐yl)tetrahydrofuran‐2‐yl)ethyl)‐7a‐methyloctahydro‐4h‐	NOUN
eurjchem-1602	2	10	inden‐4‐one	inden‐4‐one	NUM
eurjchem-1602	2	11	modou	modou	NOUN
eurjchem-1602	2	12	lo	lo	PROPN
eurjchem-1602	2	13	1	1	NUM
eurjchem-1602	2	14	,	,	PUNCT
eurjchem-1602	2	15	andrea	andrea	PROPN
eurjchem-1602	2	16	martínez	martínez	PROPN
eurjchem-1602	2	17	2	2	NUM
eurjchem-1602	2	18	,	,	PUNCT
eurjchem-1602	2	19	hugo	hugo	PROPN
eurjchem-1602	2	20	santalla	santalla	NOUN
eurjchem-1602	2	21	2	2	NUM
eurjchem-1602	2	22	,	,	PUNCT
eurjchem-1602	2	23	fátima	fátima	PROPN
eurjchem-1602	2	24	garrido	garrido	NOUN
eurjchem-1602	2	25	2	2	NUM
eurjchem-1602	2	26	,	,	PUNCT
eurjchem-1602	2	27	aliou	aliou	ADJ
eurjchem-1602	2	28	hamady	hamady	PROPN
eurjchem-1602	2	29	barry	barry	PROPN
eurjchem-1602	2	30	3	3	NUM
eurjchem-1602	2	31	and	and	CCONJ
eurjchem-1602	2	32	mohamed	mohamed	PROPN
eurjchem-1602	2	33	gaye	gaye	PROPN
eurjchem-1602	2	34	1	1	NUM
eurjchem-1602	2	35	,	,	PUNCT
eurjchem-1602	2	36	*	*	PROPN
eurjchem-1602	2	37	1	1	NUM
eurjchem-1602	2	38	department	department	NOUN
eurjchem-1602	2	39	of	of	ADP
eurjchem-1602	2	40	chemistry	chemistry	NOUN
eurjchem-1602	2	41	,	,	PUNCT
eurjchem-1602	2	42	university	university	NOUN
eurjchem-1602	2	43	cheikh	cheikh	PROPN
eurjchem-1602	2	44	anta	anta	PROPN
eurjchem-1602	2	45	diop	diop	PROPN
eurjchem-1602	2	46	,	,	PUNCT
eurjchem-1602	2	47	dakar	dakar	NOUN
eurjchem-1602	2	48	,	,	PUNCT
eurjchem-1602	2	49	10700	10700	NUM
eurjchem-1602	2	50	,	,	PUNCT
eurjchem-1602	2	51	senegal	senegal	NOUN
eurjchem-1602	2	52	2	2	NUM
eurjchem-1602	2	53	dipartamento	dipartamento	PROPN
eurjchem-1602	2	54	química	química	PROPN
eurjchem-1602	2	55	orgínica	orgínica	PROPN
eurjchem-1602	2	56	,	,	PUNCT
eurjchem-1602	2	57	facultade	facultade	PROPN
eurjchem-1602	2	58	de	de	PROPN
eurjchem-1602	2	59	química	química	PROPN
eurjchem-1602	2	60	,	,	PUNCT
eurjchem-1602	2	61	universidade	universidade	PROPN
eurjchem-1602	2	62	de	de	PROPN
eurjchem-1602	2	63	vigo	vigo	PROPN
eurjchem-1602	2	64	,	,	PUNCT
eurjchem-1602	2	65	vigo	vigo	PROPN
eurjchem-1602	2	66	,	,	PUNCT
eurjchem-1602	2	67	36310	36310	NUM
eurjchem-1602	2	68	,	,	PUNCT
eurjchem-1602	2	69	spain	spain	PROPN
eurjchem-1602	2	70	3	3	NUM
eurjchem-1602	2	71	department	department	PROPN
eurjchem-1602	2	72	of	of	ADP
eurjchem-1602	2	73	chemistry	chemistry	NOUN
eurjchem-1602	2	74	,	,	PUNCT
eurjchem-1602	2	75	university	university	PROPN
eurjchem-1602	2	76	of	of	ADP
eurjchem-1602	2	77	nouakchott	nouakchott	PROPN
eurjchem-1602	2	78	,	,	PUNCT
eurjchem-1602	2	79	nouakchott	nouakchott	PROPN
eurjchem-1602	2	80	,	,	PUNCT
eurjchem-1602	2	81	130301	130301	NUM
eurjchem-1602	2	82	,	,	PUNCT
eurjchem-1602	2	83	mauritania	mauritania	NOUN
eurjchem-1602	2	84	*	*	PUNCT
eurjchem-1602	2	85	corresponding	correspond	VERB
eurjchem-1602	2	86	author	author	NOUN
eurjchem-1602	2	87	at	at	ADP
eurjchem-1602	2	88	:	:	PUNCT
eurjchem-1602	2	89	department	department	NOUN
eurjchem-1602	2	90	of	of	ADP
eurjchem-1602	2	91	chemistry	chemistry	NOUN
eurjchem-1602	2	92	,	,	PUNCT
eurjchem-1602	2	93	university	university	NOUN
eurjchem-1602	2	94	cheikh	cheikh	PROPN
eurjchem-1602	2	95	anta	anta	PROPN
eurjchem-1602	2	96	diop	diop	PROPN
eurjchem-1602	2	97	,	,	PUNCT
eurjchem-1602	2	98	dakar	dakar	NOUN
eurjchem-1602	2	99	,	,	PUNCT
eurjchem-1602	2	100	10700	10700	NUM
eurjchem-1602	2	101	,	,	PUNCT
eurjchem-1602	2	102	senegal	senegal	NOUN
eurjchem-1602	2	103	.	.	PUNCT
eurjchem-1602	3	1	tel	tel	PROPN
eurjchem-1602	3	2	.	.	PUNCT
eurjchem-1602	3	3	:	:	PUNCT
eurjchem-1602	4	1	+221.77.5555891	+221.77.5555891	PROPN
eurjchem-1602	4	2	.	.	PUNCT
eurjchem-1602	5	1	fax	fax	NOUN
eurjchem-1602	5	2	:	:	PUNCT
eurjchem-1602	5	3	+221.33.8246318	+221.33.8246318	PROPN
eurjchem-1602	5	4	.	.	PUNCT
eurjchem-1602	5	5	e‐mail	e‐mail	PUNCT
eurjchem-1602	6	1	address	address	NOUN
eurjchem-1602	6	2	:	:	PUNCT
eurjchem-1602	6	3	mohamedl.gaye@ucad.edu.sn	mohamedl.gaye@ucad.edu.sn	NOUN
eurjchem-1602	6	4	(	(	PUNCT
eurjchem-1602	6	5	m.	m.	NOUN
eurjchem-1602	6	6	gaye	gaye	PROPN
eurjchem-1602	6	7	)	)	PUNCT
eurjchem-1602	6	8	.	.	PUNCT
eurjchem-1602	7	1	article	article	NOUN
eurjchem-1602	7	2	information	information	PROPN
eurjchem-1602	7	3	abstract	abstract	ADJ
eurjchem-1602	7	4	doi	doi	PROPN
eurjchem-1602	7	5	:	:	PUNCT
eurjchem-1602	7	6	 	 	SPACE
eurjchem-1602	7	7	10.5155	10.5155	NUM
eurjchem-1602	7	8	/	/	SYM
eurjchem-1602	7	9	eurjchem.8.3.248	eurjchem.8.3.248	PROPN
eurjchem-1602	7	10	-	-	PUNCT
eurjchem-1602	7	11	251.1602	251.1602	NUM
eurjchem-1602	7	12	received	receive	VERB
eurjchem-1602	7	13	:	:	PUNCT
eurjchem-1602	7	14	21	21	NUM
eurjchem-1602	7	15	june	june	PROPN
eurjchem-1602	7	16	2017	2017	NUM
eurjchem-1602	7	17	received	receive	VERB
eurjchem-1602	7	18	in	in	ADP
eurjchem-1602	7	19	revised	revise	VERB
eurjchem-1602	7	20	form	form	NOUN
eurjchem-1602	7	21	:	:	PUNCT
eurjchem-1602	7	22	12	12	NUM
eurjchem-1602	7	23	july	july	PROPN
eurjchem-1602	7	24	2017	2017	NUM
eurjchem-1602	7	25	accepted	accept	VERB
eurjchem-1602	7	26	:	:	PUNCT
eurjchem-1602	7	27	15	15	NUM
eurjchem-1602	7	28	july	july	PROPN
eurjchem-1602	7	29	2017	2017	NUM
eurjchem-1602	7	30	published	publish	VERB
eurjchem-1602	7	31	online	online	ADV
eurjchem-1602	7	32	:	:	PUNCT
eurjchem-1602	7	33	30	30	NUM
eurjchem-1602	7	34	september	september	PROPN
eurjchem-1602	7	35	2017	2017	NUM
eurjchem-1602	7	36	printed	print	VERB
eurjchem-1602	7	37	:	:	PUNCT
eurjchem-1602	7	38	30	30	NUM
eurjchem-1602	7	39	september	september	PROPN
eurjchem-1602	7	40	2017	2017	NUM
eurjchem-1602	7	41	  	  	SPACE
eurjchem-1602	7	42	the	the	DET
eurjchem-1602	7	43	crystal	crystal	NOUN
eurjchem-1602	7	44	of	of	ADP
eurjchem-1602	7	45	the	the	DET
eurjchem-1602	7	46	title	title	NOUN
eurjchem-1602	7	47	compound	compound	NOUN
eurjchem-1602	7	48	,	,	PUNCT
eurjchem-1602	7	49	c21h36o3	c21h36o3	PROPN
eurjchem-1602	7	50	contains	contain	VERB
eurjchem-1602	7	51	an	an	DET
eurjchem-1602	7	52	oxolane	oxolane	NOUN
eurjchem-1602	7	53	ring	ring	NOUN
eurjchem-1602	7	54	,	,	PUNCT
eurjchem-1602	7	55	and	and	CCONJ
eurjchem-1602	7	56	six	six	NUM
eurjchem-1602	7	57	defined	define	VERB
eurjchem-1602	7	58	stereocenters	stereocenter	NOUN
eurjchem-1602	7	59	which	which	PRON
eurjchem-1602	7	60	are	be	AUX
eurjchem-1602	7	61	unambigously	unambigously	ADV
eurjchem-1602	7	62	established	establish	VERB
eurjchem-1602	7	63	by	by	ADP
eurjchem-1602	7	64	the	the	DET
eurjchem-1602	7	65	crystallography	crystallography	NOUN
eurjchem-1602	7	66	study	study	NOUN
eurjchem-1602	7	67	.	.	PUNCT
eurjchem-1602	8	1	a	a	DET
eurjchem-1602	8	2	three	three	NUM
eurjchem-1602	8	3	dimensional	dimensional	ADJ
eurjchem-1602	8	4	supramolecular	supramolecular	ADJ
eurjchem-1602	8	5	architecture	architecture	NOUN
eurjchem-1602	8	6	is	be	AUX
eurjchem-1602	8	7	ensured	ensure	VERB
eurjchem-1602	8	8	by	by	ADP
eurjchem-1602	8	9	hydrogen	hydrogen	NOUN
eurjchem-1602	8	10	bonds	bond	NOUN
eurjchem-1602	8	11	from	from	ADP
eurjchem-1602	8	12	the	the	DET
eurjchem-1602	8	13	hydroxy	hydroxy	PROPN
eurjchem-1602	8	14	group	group	NOUN
eurjchem-1602	8	15	which	which	PRON
eurjchem-1602	8	16	is	be	AUX
eurjchem-1602	8	17	both	both	PRON
eurjchem-1602	8	18	engaged	engage	VERB
eurjchem-1602	8	19	in	in	ADP
eurjchem-1602	8	20	inter	inter	NOUN
eurjchem-1602	8	21	(	(	PUNCT
eurjchem-1602	8	22	o‐h···o2	o‐h···o2	PROPN
eurjchem-1602	8	23	)	)	PUNCT
eurjchem-1602	8	24	and	and	CCONJ
eurjchem-1602	8	25	intramolecular	intramolecular	ADJ
eurjchem-1602	8	26	c‐h···o‐h	c‐h···o‐h	NOUN
eurjchem-1602	8	27	)	)	PUNCT
eurjchem-1602	8	28	hydrogen	hydrogen	NOUN
eurjchem-1602	8	29	bonds	bond	NOUN
eurjchem-1602	8	30	.	.	PUNCT
eurjchem-1602	9	1	weak	weak	ADJ
eurjchem-1602	9	2	c‐h···o	c‐h···o	NOUN
eurjchem-1602	9	3	=	=	SYM
eurjchem-1602	9	4	c	c	NOUN
eurjchem-1602	9	5	hydrogen	hydrogen	NOUN
eurjchem-1602	9	6	bonds	bond	NOUN
eurjchem-1602	9	7	are	be	AUX
eurjchem-1602	9	8	involved	involve	VERB
eurjchem-1602	9	9	also	also	ADV
eurjchem-1602	9	10	into	into	ADP
eurjchem-1602	9	11	the	the	DET
eurjchem-1602	9	12	consolidation	consolidation	NOUN
eurjchem-1602	9	13	of	of	ADP
eurjchem-1602	9	14	the	the	DET
eurjchem-1602	9	15	network	network	NOUN
eurjchem-1602	9	16	.	.	PUNCT
eurjchem-1602	10	1	keywords	keyword	VERB
eurjchem-1602	10	2	calcitriol	calcitriol	NOUN
eurjchem-1602	10	3	vitamin	vitamin	NOUN
eurjchem-1602	10	4	d	d	PROPN
eurjchem-1602	10	5	crystal	crystal	NOUN
eurjchem-1602	10	6	structure	structure	NOUN
eurjchem-1602	10	7	nmr	nmr	NOUN
eurjchem-1602	10	8	spectroscopy	spectroscopy	NOUN
eurjchem-1602	10	9	pyridinium	pyridinium	NOUN
eurjchem-1602	10	10	dichromate	dichromate	NOUN
eurjchem-1602	10	11	heterocycle	heterocycle	NOUN
eurjchem-1602	10	12	compounds	compound	NOUN
eurjchem-1602	10	13	cite	cite	VERB
eurjchem-1602	10	14	this	this	PRON
eurjchem-1602	10	15	:	:	PUNCT
eurjchem-1602	10	16	eur	eur	PROPN
eurjchem-1602	10	17	.	.	PUNCT
eurjchem-1602	11	1	j.	j.	PROPN
eurjchem-1602	11	2	chem	chem	PROPN
eurjchem-1602	11	3	.	.	PUNCT
eurjchem-1602	12	1	2017	2017	NUM
eurjchem-1602	12	2	,	,	PUNCT
eurjchem-1602	12	3	8(3	8(3	NUM
eurjchem-1602	12	4	)	)	PUNCT
eurjchem-1602	12	5	,	,	PUNCT
eurjchem-1602	12	6	248‐251	248‐251	NUM
eurjchem-1602	12	7	1	1	NUM
eurjchem-1602	12	8	.	.	PUNCT
eurjchem-1602	13	1	introduction	introduction	NOUN
eurjchem-1602	13	2	our	our	PRON
eurjchem-1602	13	3	constant	constant	ADJ
eurjchem-1602	13	4	interest	interest	NOUN
eurjchem-1602	13	5	in	in	ADP
eurjchem-1602	13	6	the	the	DET
eurjchem-1602	13	7	chemistry	chemistry	NOUN
eurjchem-1602	13	8	of	of	ADP
eurjchem-1602	13	9	heterocyclic	heterocyclic	ADJ
eurjchem-1602	13	10	compounds	compound	NOUN
eurjchem-1602	13	11	and	and	CCONJ
eurjchem-1602	13	12	particularly	particularly	ADV
eurjchem-1602	13	13	in	in	ADP
eurjchem-1602	13	14	the	the	DET
eurjchem-1602	13	15	synthesis	synthesis	NOUN
eurjchem-1602	13	16	of	of	ADP
eurjchem-1602	13	17	vitamin	vitamin	NOUN
eurjchem-1602	13	18	d	d	NOUN
eurjchem-1602	13	19	analogues	analogue	NOUN
eurjchem-1602	13	20	,	,	PUNCT
eurjchem-1602	13	21	has	have	AUX
eurjchem-1602	13	22	led	lead	VERB
eurjchem-1602	13	23	us	we	PRON
eurjchem-1602	13	24	to	to	PART
eurjchem-1602	13	25	develop	develop	VERB
eurjchem-1602	13	26	several	several	ADJ
eurjchem-1602	13	27	methods	method	NOUN
eurjchem-1602	13	28	for	for	ADP
eurjchem-1602	13	29	the	the	DET
eurjchem-1602	13	30	synthesis	synthesis	NOUN
eurjchem-1602	13	31	of	of	ADP
eurjchem-1602	13	32	these	these	DET
eurjchem-1602	13	33	compounds	compound	NOUN
eurjchem-1602	13	34	[	[	X
eurjchem-1602	13	35	1,2	1,2	NUM
eurjchem-1602	13	36	]	]	PUNCT
eurjchem-1602	13	37	.	.	PUNCT
eurjchem-1602	14	1	we	we	PRON
eurjchem-1602	14	2	also	also	ADV
eurjchem-1602	14	3	considered	consider	VERB
eurjchem-1602	14	4	their	their	PRON
eurjchem-1602	14	5	biological	biological	ADJ
eurjchem-1602	14	6	activities	activity	NOUN
eurjchem-1602	14	7	which	which	PRON
eurjchem-1602	14	8	are	be	AUX
eurjchem-1602	14	9	studied	study	VERB
eurjchem-1602	14	10	in	in	ADP
eurjchem-1602	14	11	the	the	DET
eurjchem-1602	14	12	literature	literature	NOUN
eurjchem-1602	14	13	[	[	X
eurjchem-1602	14	14	3	3	NUM
eurjchem-1602	14	15	]	]	PUNCT
eurjchem-1602	14	16	.	.	PUNCT
eurjchem-1602	15	1	recently	recently	ADV
eurjchem-1602	15	2	,	,	PUNCT
eurjchem-1602	15	3	we	we	PRON
eurjchem-1602	15	4	reported	report	VERB
eurjchem-1602	15	5	the	the	DET
eurjchem-1602	15	6	synthesis	synthesis	NOUN
eurjchem-1602	15	7	of	of	ADP
eurjchem-1602	15	8	a	a	DET
eurjchem-1602	15	9	new	new	ADJ
eurjchem-1602	15	10	vitamin	vitamin	NOUN
eurjchem-1602	15	11	d2	d2	NOUN
eurjchem-1602	15	12	analogue	analogue	NOUN
eurjchem-1602	15	13	and	and	CCONJ
eurjchem-1602	15	14	the	the	DET
eurjchem-1602	15	15	evaluation	evaluation	NOUN
eurjchem-1602	15	16	of	of	ADP
eurjchem-1602	15	17	its	its	PRON
eurjchem-1602	15	18	biological	biological	ADJ
eurjchem-1602	15	19	activity	activity	NOUN
eurjchem-1602	15	20	on	on	ADP
eurjchem-1602	15	21	colon	colon	NOUN
eurjchem-1602	15	22	cancer	cancer	NOUN
eurjchem-1602	15	23	[	[	X
eurjchem-1602	15	24	4	4	NUM
eurjchem-1602	15	25	]	]	PUNCT
eurjchem-1602	15	26	.	.	PUNCT
eurjchem-1602	16	1	in	in	ADP
eurjchem-1602	16	2	the	the	DET
eurjchem-1602	16	3	continuation	continuation	NOUN
eurjchem-1602	16	4	of	of	ADP
eurjchem-1602	16	5	our	our	PRON
eurjchem-1602	16	6	work	work	NOUN
eurjchem-1602	16	7	on	on	ADP
eurjchem-1602	16	8	the	the	DET
eurjchem-1602	16	9	analogues	analogue	NOUN
eurjchem-1602	16	10	of	of	ADP
eurjchem-1602	16	11	vitamin	vitamin	NOUN
eurjchem-1602	16	12	d	d	NOUN
eurjchem-1602	16	13	,	,	PUNCT
eurjchem-1602	16	14	we	we	PRON
eurjchem-1602	16	15	synthesized	synthesize	VERB
eurjchem-1602	16	16	two	two	NUM
eurjchem-1602	16	17	new	new	ADJ
eurjchem-1602	16	18	molecules	molecule	NOUN
eurjchem-1602	16	19	of	of	ADP
eurjchem-1602	16	20	calcitriol	calcitriol	NOUN
eurjchem-1602	16	21	from	from	ADP
eurjchem-1602	16	22	an	an	DET
eurjchem-1602	16	23	oxolane	oxolane	NOUN
eurjchem-1602	16	24	ring	ring	NOUN
eurjchem-1602	16	25	and	and	CCONJ
eurjchem-1602	16	26	its	its	PRON
eurjchem-1602	16	27	side	side	NOUN
eurjchem-1602	16	28	chains	chain	NOUN
eurjchem-1602	16	29	[	[	X
eurjchem-1602	16	30	5	5	NUM
eurjchem-1602	16	31	]	]	PUNCT
eurjchem-1602	16	32	.	.	PUNCT
eurjchem-1602	17	1	in	in	ADP
eurjchem-1602	17	2	this	this	DET
eurjchem-1602	17	3	study	study	NOUN
eurjchem-1602	17	4	,	,	PUNCT
eurjchem-1602	17	5	we	we	PRON
eurjchem-1602	17	6	present	present	VERB
eurjchem-1602	17	7	the	the	DET
eurjchem-1602	17	8	structure	structure	NOUN
eurjchem-1602	17	9	of	of	ADP
eurjchem-1602	17	10	a	a	DET
eurjchem-1602	17	11	new	new	ADJ
eurjchem-1602	17	12	analog	analog	NOUN
eurjchem-1602	17	13	of	of	ADP
eurjchem-1602	17	14	calcitriol	calcitriol	NOUN
eurjchem-1602	17	15	with	with	ADP
eurjchem-1602	17	16	six	six	NUM
eurjchem-1602	17	17	stereo	stereo	NOUN
eurjchem-1602	17	18	centers	center	NOUN
eurjchem-1602	17	19	.	.	PUNCT
eurjchem-1602	18	1	the	the	DET
eurjchem-1602	18	2	crystal	crystal	NOUN
eurjchem-1602	18	3	structure	structure	NOUN
eurjchem-1602	18	4	allowed	allow	VERB
eurjchem-1602	18	5	elucidating	elucidate	VERB
eurjchem-1602	18	6	the	the	DET
eurjchem-1602	18	7	absolute	absolute	ADJ
eurjchem-1602	18	8	configuration	configuration	NOUN
eurjchem-1602	18	9	of	of	ADP
eurjchem-1602	18	10	the	the	DET
eurjchem-1602	18	11	stereo	stereo	NOUN
eurjchem-1602	18	12	centers	center	NOUN
eurjchem-1602	18	13	.	.	PUNCT
eurjchem-1602	19	1	2	2	X
eurjchem-1602	19	2	.	.	X
eurjchem-1602	19	3	experimental	experimental	ADJ
eurjchem-1602	19	4	2.1	2.1	NUM
eurjchem-1602	19	5	.	.	PUNCT
eurjchem-1602	19	6	materials	material	NOUN
eurjchem-1602	19	7	and	and	CCONJ
eurjchem-1602	19	8	physical	physical	ADJ
eurjchem-1602	19	9	methods	method	NOUN
eurjchem-1602	19	10	diol	diol	NOUN
eurjchem-1602	19	11	and	and	CCONJ
eurjchem-1602	19	12	pyridinium	pyridinium	PROPN
eurjchem-1602	19	13	dichromate	dichromate	PROPN
eurjchem-1602	19	14	(	(	PUNCT
eurjchem-1602	19	15	pdc	pdc	PROPN
eurjchem-1602	19	16	)	)	PUNCT
eurjchem-1602	19	17	were	be	AUX
eurjchem-1602	19	18	purchased	purchase	VERB
eurjchem-1602	19	19	from	from	ADP
eurjchem-1602	19	20	aldrich	aldrich	PROPN
eurjchem-1602	19	21	and	and	CCONJ
eurjchem-1602	19	22	used	use	VERB
eurjchem-1602	19	23	without	without	ADP
eurjchem-1602	19	24	further	further	ADJ
eurjchem-1602	19	25	purification	purification	NOUN
eurjchem-1602	19	26	.	.	PUNCT
eurjchem-1602	20	1	the	the	DET
eurjchem-1602	20	2	ir	ir	PROPN
eurjchem-1602	20	3	spectrum	spectrum	NOUN
eurjchem-1602	20	4	was	be	AUX
eurjchem-1602	20	5	recorded	record	VERB
eurjchem-1602	20	6	as	as	ADP
eurjchem-1602	20	7	kbr	kbr	PROPN
eurjchem-1602	20	8	discs	disc	NOUN
eurjchem-1602	20	9	on	on	ADP
eurjchem-1602	20	10	a	a	DET
eurjchem-1602	20	11	bruker	bruker	NOUN
eurjchem-1602	20	12	ifs‐66	ifs‐66	NUM
eurjchem-1602	20	13	v	v	NOUN
eurjchem-1602	20	14	spectrophotometer	spectrophotometer	NOUN
eurjchem-1602	20	15	(	(	PUNCT
eurjchem-1602	20	16	4000‐400	4000‐400	NUM
eurjchem-1602	20	17	cm‐1	cm‐1	NOUN
eurjchem-1602	20	18	)	)	PUNCT
eurjchem-1602	20	19	.	.	PUNCT
eurjchem-1602	21	1	mass	mass	PROPN
eurjchem-1602	21	2	spectrometry	spectrometry	NOUN
eurjchem-1602	21	3	was	be	AUX
eurjchem-1602	21	4	carried	carry	VERB
eurjchem-1602	21	5	out	out	ADP
eurjchem-1602	21	6	with	with	ADP
eurjchem-1602	21	7	a	a	DET
eurjchem-1602	21	8	hewlett	hewlett	PROPN
eurjchem-1602	21	9	packard	packard	PROPN
eurjchem-1602	21	10	5988a	5988a	NUM
eurjchem-1602	21	11	spectrometer	spectrometer	NOUN
eurjchem-1602	21	12	.	.	PUNCT
eurjchem-1602	22	1	the	the	DET
eurjchem-1602	22	2	1h	1h	NUM
eurjchem-1602	22	3	and	and	CCONJ
eurjchem-1602	22	4	13c	13c	NOUN
eurjchem-1602	22	5	nmr	nmr	NOUN
eurjchem-1602	22	6	spectra	spectra	NOUN
eurjchem-1602	22	7	of	of	ADP
eurjchem-1602	22	8	the	the	DET
eurjchem-1602	22	9	compound	compound	NOUN
eurjchem-1602	22	10	1	1	NUM
eurjchem-1602	22	11	were	be	AUX
eurjchem-1602	22	12	recorded	record	VERB
eurjchem-1602	22	13	in	in	ADP
eurjchem-1602	22	14	cdcl3	cdcl3	NOUN
eurjchem-1602	22	15	on	on	ADP
eurjchem-1602	22	16	a	a	DET
eurjchem-1602	22	17	bruker	bruker	NOUN
eurjchem-1602	22	18	500	500	NUM
eurjchem-1602	22	19	mhz	mhz	NOUN
eurjchem-1602	22	20	spectrometer	spectrometer	NOUN
eurjchem-1602	22	21	at	at	ADP
eurjchem-1602	22	22	room	room	NOUN
eurjchem-1602	22	23	tempera‐	tempera‐	PROPN
eurjchem-1602	22	24	ture	ture	PROPN
eurjchem-1602	22	25	using	use	VERB
eurjchem-1602	22	26	tms	tms	PROPN
eurjchem-1602	22	27	as	as	ADP
eurjchem-1602	22	28	internal	internal	ADJ
eurjchem-1602	22	29	reference	reference	NOUN
eurjchem-1602	22	30	.	.	PUNCT
eurjchem-1602	23	1	2.2	2.2	NUM
eurjchem-1602	23	2	.	.	PUNCT
eurjchem-1602	24	1	crystal	crystal	NOUN
eurjchem-1602	24	2	structure	structure	NOUN
eurjchem-1602	24	3	determination	determination	NOUN
eurjchem-1602	24	4	crystallographic	crystallographic	ADJ
eurjchem-1602	24	5	data	datum	NOUN
eurjchem-1602	24	6	were	be	AUX
eurjchem-1602	24	7	collected	collect	VERB
eurjchem-1602	24	8	at	at	ADP
eurjchem-1602	24	9	room	room	NOUN
eurjchem-1602	24	10	temperature	temperature	NOUN
eurjchem-1602	24	11	using	use	VERB
eurjchem-1602	24	12	a	a	DET
eurjchem-1602	24	13	bruker	bruker	ADJ
eurjchem-1602	24	14	smart	smart	ADJ
eurjchem-1602	24	15	6000	6000	NUM
eurjchem-1602	24	16	ccd	ccd	NOUN
eurjchem-1602	24	17	detector	detector	NOUN
eurjchem-1602	24	18	and	and	CCONJ
eurjchem-1602	24	19	cu‐kα	cu‐kα	NOUN
eurjchem-1602	24	20	radiation	radiation	NOUN
eurjchem-1602	24	21	(	(	PUNCT
eurjchem-1602	24	22			X
eurjchem-1602	24	23	=	=	X
eurjchem-1602	24	24	1.54178	1.54178	NUM
eurjchem-1602	24	25	å	å	NOUN
eurjchem-1602	24	26	)	)	PUNCT
eurjchem-1602	24	27	generated	generate	VERB
eurjchem-1602	24	28	by	by	ADP
eurjchem-1602	24	29	a	a	DET
eurjchem-1602	24	30	incoatec	incoatec	ADJ
eurjchem-1602	24	31	microfocus	microfocus	NOUN
eurjchem-1602	24	32	sour‐	sour‐	PROPN
eurjchem-1602	24	33	ce	ce	PROPN
eurjchem-1602	24	34	equipped	equip	VERB
eurjchem-1602	24	35	with	with	ADP
eurjchem-1602	24	36	incoatec	incoatec	ADJ
eurjchem-1602	24	37	quazar	quazar	PROPN
eurjchem-1602	24	38	mx	mx	PROPN
eurjchem-1602	24	39	optics	optic	NOUN
eurjchem-1602	24	40	.	.	PUNCT
eurjchem-1602	25	1	the	the	DET
eurjchem-1602	25	2	software	software	NOUN
eurjchem-1602	25	3	apex3	apex3	PUNCT
eurjchem-1602	26	1	[	[	X
eurjchem-1602	26	2	6	6	NUM
eurjchem-1602	26	3	]	]	PUNCT
eurjchem-1602	26	4	was	be	AUX
eurjchem-1602	26	5	used	use	VERB
eurjchem-1602	26	6	for	for	ADP
eurjchem-1602	26	7	collecting	collect	VERB
eurjchem-1602	26	8	frames	frame	NOUN
eurjchem-1602	26	9	of	of	ADP
eurjchem-1602	26	10	data	datum	NOUN
eurjchem-1602	26	11	,	,	PUNCT
eurjchem-1602	26	12	indexing	indexing	NOUN
eurjchem-1602	26	13	reflections	reflection	NOUN
eurjchem-1602	26	14	and	and	CCONJ
eurjchem-1602	26	15	the	the	DET
eurjchem-1602	26	16	determination	determination	NOUN
eurjchem-1602	26	17	of	of	ADP
eurjchem-1602	26	18	lattice	lattice	NOUN
eurjchem-1602	26	19	parameters	parameter	NOUN
eurjchem-1602	26	20	,	,	PUNCT
eurjchem-1602	26	21	saint	saint	PROPN
eurjchem-1602	27	1	[	[	X
eurjchem-1602	27	2	6	6	NUM
eurjchem-1602	27	3	]	]	PUNCT
eurjchem-1602	27	4	for	for	ADP
eurjchem-1602	27	5	integration	integration	NOUN
eurjchem-1602	27	6	of	of	ADP
eurjchem-1602	27	7	intensity	intensity	NOUN
eurjchem-1602	27	8	of	of	ADP
eurjchem-1602	27	9	reflections	reflection	NOUN
eurjchem-1602	27	10	,	,	PUNCT
eurjchem-1602	27	11	and	and	CCONJ
eurjchem-1602	27	12	sadabs	sadab	NOUN
eurjchem-1602	28	1	[	[	X
eurjchem-1602	28	2	6	6	NUM
eurjchem-1602	28	3	]	]	PUNCT
eurjchem-1602	28	4	for	for	ADP
eurjchem-1602	28	5	scaling	scaling	NOUN
eurjchem-1602	28	6	and	and	CCONJ
eurjchem-1602	28	7	empirical	empirical	ADJ
eurjchem-1602	28	8	absorption	absorption	NOUN
eurjchem-1602	28	9	correction	correction	NOUN
eurjchem-1602	28	10	.	.	PUNCT
eurjchem-1602	29	1	the	the	DET
eurjchem-1602	29	2	structure	structure	NOUN
eurjchem-1602	29	3	was	be	AUX
eurjchem-1602	29	4	solved	solve	VERB
eurjchem-1602	29	5	by	by	ADP
eurjchem-1602	29	6	dual‐space	dual‐space	NOUN
eurjchem-1602	29	7	methods	method	NOUN
eurjchem-1602	29	8	using	use	VERB
eurjchem-1602	29	9	the	the	DET
eurjchem-1602	29	10	program	program	NOUN
eurjchem-1602	29	11	shelxt	shelxt	NOUN
eurjchem-1602	29	12	[	[	X
eurjchem-1602	29	13	7	7	NUM
eurjchem-1602	29	14	]	]	PUNCT
eurjchem-1602	29	15	.	.	PUNCT
eurjchem-1602	30	1	lo	lo	PROPN
eurjchem-1602	30	2	et	et	PROPN
eurjchem-1602	30	3	al	al	PROPN
eurjchem-1602	30	4	.	.	PUNCT
eurjchem-1602	30	5	/	/	SYM
eurjchem-1602	30	6	european	european	PROPN
eurjchem-1602	30	7	journal	journal	PROPN
eurjchem-1602	30	8	of	of	ADP
eurjchem-1602	30	9	chemistry	chemistry	NOUN
eurjchem-1602	30	10	8	8	NUM
eurjchem-1602	30	11	(	(	PUNCT
eurjchem-1602	30	12	3	3	NUM
eurjchem-1602	30	13	)	)	PUNCT
eurjchem-1602	30	14	(	(	PUNCT
eurjchem-1602	30	15	2017	2017	NUM
eurjchem-1602	30	16	)	)	PUNCT
eurjchem-1602	30	17	248‐251	248‐251	PROPN
eurjchem-1602	30	18	249	249	NUM
eurjchem-1602	30	19	scheme	scheme	NOUN
eurjchem-1602	30	20	1	1	NUM
eurjchem-1602	30	21	figure	figure	NOUN
eurjchem-1602	30	22	1	1	NUM
eurjchem-1602	30	23	.	.	PUNCT
eurjchem-1602	30	24	crystal	crystal	NOUN
eurjchem-1602	30	25	structure	structure	NOUN
eurjchem-1602	30	26	of	of	ADP
eurjchem-1602	30	27	the	the	DET
eurjchem-1602	30	28	compound	compound	NOUN
eurjchem-1602	30	29	1	1	NUM
eurjchem-1602	30	30	.	.	PUNCT
eurjchem-1602	31	1	all	all	DET
eurjchem-1602	31	2	non‐hydrogen	non‐hydrogen	DET
eurjchem-1602	31	3	atoms	atom	NOUN
eurjchem-1602	31	4	were	be	AUX
eurjchem-1602	31	5	refined	refine	VERB
eurjchem-1602	31	6	with	with	ADP
eurjchem-1602	31	7	anisotropic	anisotropic	NOUN
eurjchem-1602	31	8	thermal	thermal	ADJ
eurjchem-1602	31	9	parameters	parameter	NOUN
eurjchem-1602	31	10	by	by	ADP
eurjchem-1602	31	11	full‐matrix	full‐matrix	NOUN
eurjchem-1602	31	12	least‐squares	least‐square	VERB
eurjchem-1602	31	13	calculations	calculation	NOUN
eurjchem-1602	31	14	on	on	ADP
eurjchem-1602	31	15	f2	f2	PROPN
eurjchem-1602	31	16	using	use	VERB
eurjchem-1602	31	17	the	the	DET
eurjchem-1602	31	18	program	program	NOUN
eurjchem-1602	31	19	shelxl	shelxl	NOUN
eurjchem-1602	31	20	[	[	X
eurjchem-1602	31	21	8	8	NUM
eurjchem-1602	31	22	]	]	PUNCT
eurjchem-1602	31	23	.	.	PUNCT
eurjchem-1602	32	1	hydrogen	hydrogen	NOUN
eurjchem-1602	32	2	atoms	atom	NOUN
eurjchem-1602	32	3	were	be	AUX
eurjchem-1602	32	4	inserted	insert	VERB
eurjchem-1602	32	5	at	at	ADP
eurjchem-1602	32	6	calculated	calculate	VERB
eurjchem-1602	32	7	positions	position	NOUN
eurjchem-1602	32	8	and	and	CCONJ
eurjchem-1602	32	9	constrained	constrain	VERB
eurjchem-1602	32	10	with	with	ADP
eurjchem-1602	32	11	isotropic	isotropic	ADJ
eurjchem-1602	32	12	thermal	thermal	ADJ
eurjchem-1602	32	13	parameters	parameter	NOUN
eurjchem-1602	32	14	except	except	SCONJ
eurjchem-1602	32	15	for	for	ADP
eurjchem-1602	32	16	the	the	DET
eurjchem-1602	32	17	hydrogen	hydrogen	NOUN
eurjchem-1602	32	18	atom	atom	NOUN
eurjchem-1602	32	19	of	of	ADP
eurjchem-1602	32	20	the	the	DET
eurjchem-1602	32	21	hydroxyl	hydroxyl	NOUN
eurjchem-1602	32	22	group	group	NOUN
eurjchem-1602	32	23	.	.	PUNCT
eurjchem-1602	33	1	drawings	drawing	NOUN
eurjchem-1602	33	2	were	be	AUX
eurjchem-1602	33	3	produced	produce	VERB
eurjchem-1602	33	4	with	with	ADP
eurjchem-1602	33	5	platon	platon	PROPN
eurjchem-1602	33	6	[	[	X
eurjchem-1602	33	7	9	9	NUM
eurjchem-1602	33	8	]	]	PUNCT
eurjchem-1602	33	9	.	.	PUNCT
eurjchem-1602	34	1	2.3	2.3	NUM
eurjchem-1602	34	2	.	.	PUNCT
eurjchem-1602	34	3	synthesis	synthesis	NOUN
eurjchem-1602	34	4	of	of	ADP
eurjchem-1602	34	5	compound	compound	NOUN
eurjchem-1602	34	6	1	1	NUM
eurjchem-1602	34	7	to	to	ADP
eurjchem-1602	34	8	a	a	DET
eurjchem-1602	34	9	solution	solution	NOUN
eurjchem-1602	34	10	of	of	ADP
eurjchem-1602	34	11	diol	diol	NOUN
eurjchem-1602	34	12	(	(	PUNCT
eurjchem-1602	34	13	2	2	NUM
eurjchem-1602	34	14	)	)	PUNCT
eurjchem-1602	34	15	(	(	PUNCT
eurjchem-1602	34	16	0.18	0.18	NUM
eurjchem-1602	34	17	mmol	mmol	NOUN
eurjchem-1602	34	18	)	)	PUNCT
eurjchem-1602	34	19	in	in	ADP
eurjchem-1602	34	20	ch2cl2	ch2cl2	PUNCT
eurjchem-1602	34	21	(	(	PUNCT
eurjchem-1602	34	22	5	5	NUM
eurjchem-1602	34	23	ml	ml	NOUN
eurjchem-1602	34	24	)	)	PUNCT
eurjchem-1602	34	25	,	,	PUNCT
eurjchem-1602	34	26	pyridinium	pyridinium	PROPN
eurjchem-1602	34	27	dichromate	dichromate	PROPN
eurjchem-1602	34	28	(	(	PUNCT
eurjchem-1602	34	29	pdc	pdc	PROPN
eurjchem-1602	34	30	)	)	PUNCT
eurjchem-1602	34	31	(	(	PUNCT
eurjchem-1602	34	32	0.37	0.37	NUM
eurjchem-1602	34	33	mmol	mmol	NOUN
eurjchem-1602	34	34	)	)	PUNCT
eurjchem-1602	34	35	was	be	AUX
eurjchem-1602	34	36	added	add	VERB
eurjchem-1602	34	37	and	and	CCONJ
eurjchem-1602	34	38	the	the	DET
eurjchem-1602	34	39	mixture	mixture	NOUN
eurjchem-1602	34	40	stirred	stir	VERB
eurjchem-1602	34	41	at	at	ADP
eurjchem-1602	34	42	room	room	NOUN
eurjchem-1602	34	43	temperature	temperature	NOUN
eurjchem-1602	34	44	for	for	ADP
eurjchem-1602	34	45	12	12	NUM
eurjchem-1602	34	46	h	h	NOUN
eurjchem-1602	34	47	,	,	PUNCT
eurjchem-1602	34	48	then	then	ADV
eurjchem-1602	34	49	the	the	DET
eurjchem-1602	34	50	solvent	solvent	NOUN
eurjchem-1602	34	51	was	be	AUX
eurjchem-1602	34	52	evaporated	evaporate	VERB
eurjchem-1602	34	53	and	and	CCONJ
eurjchem-1602	34	54	the	the	DET
eurjchem-1602	34	55	residue	residue	NOUN
eurjchem-1602	34	56	was	be	AUX
eurjchem-1602	34	57	chromatographed	chromatographe	VERB
eurjchem-1602	34	58	on	on	ADP
eurjchem-1602	34	59	sılica	sılica	NOUN
eurjchem-1602	34	60	gel	gel	NOUN
eurjchem-1602	34	61	using	use	VERB
eurjchem-1602	34	62	(	(	PUNCT
eurjchem-1602	34	63	10	10	NUM
eurjchem-1602	34	64	%	%	NOUN
eurjchem-1602	34	65	,	,	PUNCT
eurjchem-1602	34	66	etoac	etoac	ADJ
eurjchem-1602	34	67	:	:	PUNCT
eurjchem-1602	34	68	hexane	hexane	ADJ
eurjchem-1602	34	69	,	,	PUNCT
eurjchem-1602	34	70	v	v	NOUN
eurjchem-1602	34	71	:	:	SYM
eurjchem-1602	34	72	v	v	NOUN
eurjchem-1602	34	73	)	)	PUNCT
eurjchem-1602	34	74	to	to	PART
eurjchem-1602	34	75	afford	afford	VERB
eurjchem-1602	34	76	ketone	ketone	NOUN
eurjchem-1602	34	77	(	(	PUNCT
eurjchem-1602	34	78	1	1	NUM
eurjchem-1602	34	79	)	)	PUNCT
eurjchem-1602	34	80	(	(	PUNCT
eurjchem-1602	34	81	scheme	scheme	NOUN
eurjchem-1602	34	82	1	1	NUM
eurjchem-1602	34	83	)	)	PUNCT
eurjchem-1602	34	84	.	.	PUNCT
eurjchem-1602	35	1	the	the	DET
eurjchem-1602	35	2	title	title	NOUN
eurjchem-1602	35	3	compound	compound	NOUN
eurjchem-1602	35	4	was	be	AUX
eurjchem-1602	35	5	recrystallized	recrystallize	VERB
eurjchem-1602	35	6	using	use	VERB
eurjchem-1602	35	7	a	a	DET
eurjchem-1602	35	8	mixture	mixture	NOUN
eurjchem-1602	35	9	of	of	ADP
eurjchem-1602	35	10	hexane	hexane	NOUN
eurjchem-1602	35	11	:	:	PUNCT
eurjchem-1602	35	12	ethyl	ethyl	PROPN
eurjchem-1602	35	13	ether	ether	NOUN
eurjchem-1602	35	14	(	(	PUNCT
eurjchem-1602	35	15	1:1	1:1	NUM
eurjchem-1602	35	16	,	,	PUNCT
eurjchem-1602	35	17	v	v	NOUN
eurjchem-1602	35	18	:	:	PUNCT
eurjchem-1602	35	19	v	v	NOUN
eurjchem-1602	35	20	)	)	PUNCT
eurjchem-1602	35	21	.	.	PUNCT
eurjchem-1602	36	1	(	(	PUNCT
eurjchem-1602	36	2	1r	1r	NUM
eurjchem-1602	36	3	,	,	PUNCT
eurjchem-1602	36	4	3ar	3ar	ADJ
eurjchem-1602	36	5	,	,	PUNCT
eurjchem-1602	36	6	7ar)‐1‐((s)‐1‐((2r	7ar)‐1‐((s)‐1‐((2r	NUM
eurjchem-1602	36	7	,	,	PUNCT
eurjchem-1602	36	8	5s)‐5‐(3‐hydroxypentan‐3‐	5s)‐5‐(3‐hydroxypentan‐3‐	NUM
eurjchem-1602	36	9	yl)tetrahydrofuran‐2‐yl)ethyl)‐7a‐methyloctahydro‐4h‐inden‐	yl)tetrahydrofuran‐2‐yl)ethyl)‐7a‐methyloctahydro‐4h‐inden‐	NOUN
eurjchem-1602	36	10	4‐one	4‐one	NOUN
eurjchem-1602	36	11	(	(	PUNCT
eurjchem-1602	36	12	1	1	NUM
eurjchem-1602	36	13	):	):	PUNCT
eurjchem-1602	36	14	color	color	NOUN
eurjchem-1602	36	15	:	:	PUNCT
eurjchem-1602	36	16	white	white	PROPN
eurjchem-1602	36	17	solid	solid	ADJ
eurjchem-1602	36	18	.	.	PUNCT
eurjchem-1602	37	1	m.p	m.p	NOUN
eurjchem-1602	37	2	:	:	PUNCT
eurjchem-1602	37	3	80‐82	80‐82	NUM
eurjchem-1602	37	4	°	°	ADP
eurjchem-1602	37	5	c	c	X
eurjchem-1602	37	6	.	.	PUNCT
eurjchem-1602	37	7	yield	yield	NOUN
eurjchem-1602	37	8	:	:	PUNCT
eurjchem-1602	37	9	88	88	NUM
eurjchem-1602	37	10	%	%	NOUN
eurjchem-1602	37	11	.	.	PUNCT
eurjchem-1602	38	1	rf	rf	VERB
eurjchem-1602	38	2	:	:	PUNCT
eurjchem-1602	38	3	0.42	0.42	NUM
eurjchem-1602	38	4	(	(	PUNCT
eurjchem-1602	38	5	30	30	NUM
eurjchem-1602	38	6	%	%	NOUN
eurjchem-1602	38	7	,	,	PUNCT
eurjchem-1602	38	8	etoac	etoac	ADJ
eurjchem-1602	38	9	:	:	PUNCT
eurjchem-1602	38	10	hexane	hexane	ADJ
eurjchem-1602	38	11	,	,	PUNCT
eurjchem-1602	38	12	v	v	NOUN
eurjchem-1602	38	13	:	:	PUNCT
eurjchem-1602	38	14	v	v	NOUN
eurjchem-1602	38	15	)	)	PUNCT
eurjchem-1602	38	16	.	.	PUNCT
eurjchem-1602	39	1	[	[	X
eurjchem-1602	39	2	α]d19	α]d19	X
eurjchem-1602	39	3	=	=	SYM
eurjchem-1602	39	4	+26.27	+26.27	PROPN
eurjchem-1602	39	5	(	(	PUNCT
eurjchem-1602	39	6	c	c	NOUN
eurjchem-1602	39	7	1.0	1.0	NUM
eurjchem-1602	39	8	,	,	PUNCT
eurjchem-1602	39	9	cdcl3	cdcl3	PROPN
eurjchem-1602	39	10	)	)	PUNCT
eurjchem-1602	39	11	.	.	PUNCT
eurjchem-1602	40	1	1h	1h	NUM
eurjchem-1602	40	2	nmr	nmr	NOUN
eurjchem-1602	40	3	(	(	PUNCT
eurjchem-1602	40	4	250	250	NUM
eurjchem-1602	40	5	mhz	mhz	NOUN
eurjchem-1602	40	6	,	,	PUNCT
eurjchem-1602	40	7	cdcl3	cdcl3	PROPN
eurjchem-1602	40	8	,	,	PUNCT
eurjchem-1602	40	9	δ	δ	PROPN
eurjchem-1602	40	10	,	,	PUNCT
eurjchem-1602	40	11	ppm	ppm	NUM
eurjchem-1602	40	12	):	):	PUNCT
eurjchem-1602	40	13	3.99	3.99	NUM
eurjchem-1602	40	14	(	(	PUNCT
eurjchem-1602	40	15	1h	1h	NUM
eurjchem-1602	40	16	,	,	PUNCT
eurjchem-1602	40	17	td	td	PROPN
eurjchem-1602	40	18	,	,	PUNCT
eurjchem-1602	40	19	j	j	PROPN
eurjchem-1602	40	20	=	=	NOUN
eurjchem-1602	40	21	10.1	10.1	NUM
eurjchem-1602	40	22	,	,	PUNCT
eurjchem-1602	40	23	5	5	NUM
eurjchem-1602	40	24	hz	hz	NOUN
eurjchem-1602	40	25	,	,	PUNCT
eurjchem-1602	40	26	h‐	h‐	PROPN
eurjchem-1602	40	27	5	5	NUM
eurjchem-1602	40	28	'	'	NUM
eurjchem-1602	40	29	)	)	PUNCT
eurjchem-1602	40	30	,	,	PUNCT
eurjchem-1602	40	31	3.81	3.81	NUM
eurjchem-1602	40	32	(	(	PUNCT
eurjchem-1602	40	33	1h	1h	NUM
eurjchem-1602	40	34	,	,	PUNCT
eurjchem-1602	40	35	dd	dd	NOUN
eurjchem-1602	40	36	,	,	PUNCT
eurjchem-1602	40	37	j	j	PROPN
eurjchem-1602	40	38	=	=	SYM
eurjchem-1602	40	39	9.8	9.8	NUM
eurjchem-1602	40	40	,	,	PUNCT
eurjchem-1602	40	41	5.7	5.7	NUM
eurjchem-1602	40	42	hz	hz	NOUN
eurjchem-1602	40	43	,	,	PUNCT
eurjchem-1602	40	44	h‐2	h‐2	NOUN
eurjchem-1602	40	45	'	'	PUNCT
eurjchem-1602	40	46	)	)	PUNCT
eurjchem-1602	40	47	,	,	PUNCT
eurjchem-1602	40	48	2.42	2.42	NUM
eurjchem-1602	40	49	(	(	PUNCT
eurjchem-1602	40	50	1h	1h	NUM
eurjchem-1602	40	51	,	,	PUNCT
eurjchem-1602	40	52	dd	dd	NOUN
eurjchem-1602	40	53	,	,	PUNCT
eurjchem-1602	40	54	j	j	PROPN
eurjchem-1602	41	1	=	=	NOUN
eurjchem-1602	41	2	11.2	11.2	NUM
eurjchem-1602	41	3	,	,	PUNCT
eurjchem-1602	41	4	7.4	7.4	NUM
eurjchem-1602	41	5	hz	hz	NOUN
eurjchem-1602	41	6	,	,	PUNCT
eurjchem-1602	41	7	h‐3a	h‐3a	PROPN
eurjchem-1602	41	8	)	)	PUNCT
eurjchem-1602	41	9	,	,	PUNCT
eurjchem-1602	41	10	2.37‐1.70	2.37‐1.70	NUM
eurjchem-1602	41	11	(	(	PUNCT
eurjchem-1602	41	12	12h	12h	NUM
eurjchem-1602	41	13	,	,	PUNCT
eurjchem-1602	41	14	m	m	PROPN
eurjchem-1602	41	15	,	,	PUNCT
eurjchem-1602	41	16	6	6	NUM
eurjchem-1602	41	17	x	x	SYM
eurjchem-1602	41	18	ch2	ch2	PROPN
eurjchem-1602	41	19	)	)	PUNCT
eurjchem-1602	41	20	,	,	PUNCT
eurjchem-1602	42	1	1.69‐1.24	1.69‐1.24	NUM
eurjchem-1602	42	2	(	(	PUNCT
eurjchem-1602	42	3	9h	9h	NUM
eurjchem-1602	42	4	,	,	PUNCT
eurjchem-1602	42	5	m	m	PRON
eurjchem-1602	42	6	,	,	PUNCT
eurjchem-1602	42	7	3	3	NUM
eurjchem-1602	42	8	x	x	SYM
eurjchem-1602	42	9	ch2	ch2	PROPN
eurjchem-1602	42	10	+	+	CCONJ
eurjchem-1602	42	11	h‐1	h‐1	PROPN
eurjchem-1602	42	12	+	+	CCONJ
eurjchem-1602	42	13	h‐1	h‐1	PROPN
eurjchem-1602	42	14	'	'	PART
eurjchem-1602	42	15	+	+	ADJ
eurjchem-1602	42	16	ho	ho	ADJ
eurjchem-1602	42	17	)	)	PUNCT
eurjchem-1602	42	18	,	,	PUNCT
eurjchem-1602	42	19	0.93	0.93	NUM
eurjchem-1602	42	20	(	(	PUNCT
eurjchem-1602	42	21	3h	3h	NUM
eurjchem-1602	42	22	,	,	PUNCT
eurjchem-1602	42	23	d	d	PROPN
eurjchem-1602	42	24	,	,	PUNCT
eurjchem-1602	42	25	j	j	PROPN
eurjchem-1602	42	26	=	=	SYM
eurjchem-1602	42	27	6.7	6.7	NUM
eurjchem-1602	42	28	hz	hz	VERB
eurjchem-1602	42	29	,	,	PUNCT
eurjchem-1602	42	30	ch3‐21	ch3‐21	PROPN
eurjchem-1602	42	31	)	)	PUNCT
eurjchem-1602	42	32	,	,	PUNCT
eurjchem-1602	42	33	0.87	0.87	NUM
eurjchem-1602	42	34	(	(	PUNCT
eurjchem-1602	42	35	6h	6h	NOUN
eurjchem-1602	42	36	,	,	PUNCT
eurjchem-1602	42	37	td	td	PROPN
eurjchem-1602	42	38	,	,	PUNCT
eurjchem-1602	42	39	j	j	PROPN
eurjchem-1602	42	40	=	=	SYM
eurjchem-1602	42	41	7.5	7.5	NUM
eurjchem-1602	42	42	,	,	PUNCT
eurjchem-1602	42	43	5.3	5.3	NUM
eurjchem-1602	42	44	hz	hz	NOUN
eurjchem-1602	42	45	,	,	PUNCT
eurjchem-1602	42	46	ch3‐et	ch3‐et	NUM
eurjchem-1602	42	47	)	)	PUNCT
eurjchem-1602	42	48	,	,	PUNCT
eurjchem-1602	42	49	0.66	0.66	NUM
eurjchem-1602	42	50	(	(	PUNCT
eurjchem-1602	42	51	3h	3h	NUM
eurjchem-1602	42	52	,	,	PUNCT
eurjchem-1602	42	53	s	s	X
eurjchem-1602	42	54	,	,	PUNCT
eurjchem-1602	42	55	ch3‐18	ch3‐18	PROPN
eurjchem-1602	42	56	)	)	PUNCT
eurjchem-1602	42	57	.	.	PUNCT
eurjchem-1602	43	1	13c	13c	NOUN
eurjchem-1602	43	2	nmr	nmr	NOUN
eurjchem-1602	43	3	(	(	PUNCT
eurjchem-1602	43	4	62.5	62.5	NUM
eurjchem-1602	43	5	mhz	mhz	NOUN
eurjchem-1602	43	6	,	,	PUNCT
eurjchem-1602	43	7	cdcl3	cdcl3	PROPN
eurjchem-1602	43	8	,	,	PUNCT
eurjchem-1602	43	9	δ	δ	PROPN
eurjchem-1602	43	10	,	,	PUNCT
eurjchem-1602	43	11	ppm	ppm	NOUN
eurjchem-1602	43	12	):	):	PUNCT
eurjchem-1602	43	13	211.91	211.91	NUM
eurjchem-1602	43	14	(	(	PUNCT
eurjchem-1602	43	15	c	c	NOUN
eurjchem-1602	43	16	=	=	NOUN
eurjchem-1602	43	17	o	o	NOUN
eurjchem-1602	43	18	)	)	PUNCT
eurjchem-1602	43	19	,	,	PUNCT
eurjchem-1602	43	20	83.49	83.49	NUM
eurjchem-1602	43	21	(	(	PUNCT
eurjchem-1602	43	22	ch‐2	ch‐2	NOUN
eurjchem-1602	43	23	'	'	PUNCT
eurjchem-1602	43	24	)	)	PUNCT
eurjchem-1602	43	25	,	,	PUNCT
eurjchem-1602	43	26	81.78	81.78	NUM
eurjchem-1602	43	27	(	(	PUNCT
eurjchem-1602	43	28	ch‐5	ch‐5	NOUN
eurjchem-1602	43	29	'	'	PUNCT
eurjchem-1602	43	30	)	)	PUNCT
eurjchem-1602	43	31	,	,	PUNCT
eurjchem-1602	43	32	74.76	74.76	NUM
eurjchem-1602	43	33	(	(	PUNCT
eurjchem-1602	43	34	c‐3	c‐3	NOUN
eurjchem-1602	43	35	''	''	PUNCT
eurjchem-1602	43	36	)	)	PUNCT
eurjchem-1602	43	37	,	,	PUNCT
eurjchem-1602	43	38	61.43	61.43	NUM
eurjchem-1602	43	39	(	(	PUNCT
eurjchem-1602	43	40	ch‐14	ch‐14	PROPN
eurjchem-1602	43	41	)	)	PUNCT
eurjchem-1602	43	42	,	,	PUNCT
eurjchem-1602	43	43	54.23	54.23	NUM
eurjchem-1602	43	44	(	(	PUNCT
eurjchem-1602	43	45	ch‐17	ch‐17	ADJ
eurjchem-1602	43	46	)	)	PUNCT
eurjchem-1602	43	47	,	,	PUNCT
eurjchem-1602	43	48	50.30	50.30	NUM
eurjchem-1602	43	49	(	(	PUNCT
eurjchem-1602	43	50	ch‐13	ch‐13	PROPN
eurjchem-1602	43	51	)	)	PUNCT
eurjchem-1602	43	52	,	,	PUNCT
eurjchem-1602	43	53	41.02	41.02	NUM
eurjchem-1602	43	54	(	(	PUNCT
eurjchem-1602	43	55	ch2	ch2	PROPN
eurjchem-1602	43	56	)	)	PUNCT
eurjchem-1602	43	57	,	,	PUNCT
eurjchem-1602	43	58	38.94	38.94	NUM
eurjchem-1602	43	59	(	(	PUNCT
eurjchem-1602	43	60	ch2	ch2	PROPN
eurjchem-1602	43	61	)	)	PUNCT
eurjchem-1602	43	62	,	,	PUNCT
eurjchem-1602	43	63	38.93	38.93	NUM
eurjchem-1602	43	64	(	(	PUNCT
eurjchem-1602	43	65	ch‐20	ch‐20	NOUN
eurjchem-1602	43	66	)	)	PUNCT
eurjchem-1602	43	67	,	,	PUNCT
eurjchem-1602	43	68	28.79	28.79	NUM
eurjchem-1602	43	69	(	(	PUNCT
eurjchem-1602	43	70	ch2	ch2	PROPN
eurjchem-1602	43	71	)	)	PUNCT
eurjchem-1602	43	72	,	,	PUNCT
eurjchem-1602	43	73	26.91	26.91	NUM
eurjchem-1602	43	74	(	(	PUNCT
eurjchem-1602	43	75	ch2	ch2	PROPN
eurjchem-1602	43	76	)	)	PUNCT
eurjchem-1602	43	77	,	,	PUNCT
eurjchem-1602	43	78	26.35	26.35	NUM
eurjchem-1602	43	79	(	(	PUNCT
eurjchem-1602	43	80	ch2	ch2	PROPN
eurjchem-1602	43	81	)	)	PUNCT
eurjchem-1602	43	82	,	,	PUNCT
eurjchem-1602	43	83	25.92	25.92	NUM
eurjchem-1602	43	84	(	(	PUNCT
eurjchem-1602	43	85	ch2	ch2	PROPN
eurjchem-1602	43	86	)	)	PUNCT
eurjchem-1602	43	87	,	,	PUNCT
eurjchem-1602	43	88	25.89	25.89	NUM
eurjchem-1602	43	89	(	(	PUNCT
eurjchem-1602	43	90	ch2	ch2	PROPN
eurjchem-1602	43	91	)	)	PUNCT
eurjchem-1602	43	92	,	,	PUNCT
eurjchem-1602	43	93	24.05	24.05	NUM
eurjchem-1602	43	94	(	(	PUNCT
eurjchem-1602	43	95	ch2	ch2	PROPN
eurjchem-1602	43	96	)	)	PUNCT
eurjchem-1602	43	97	,	,	PUNCT
eurjchem-1602	43	98	19.26	19.26	NUM
eurjchem-1602	43	99	(	(	PUNCT
eurjchem-1602	43	100	ch2	ch2	PROPN
eurjchem-1602	43	101	)	)	PUNCT
eurjchem-1602	43	102	,	,	PUNCT
eurjchem-1602	43	103	12.69	12.69	NUM
eurjchem-1602	43	104	(	(	PUNCT
eurjchem-1602	43	105	ch3‐21	ch3‐21	NUM
eurjchem-1602	43	106	)	)	PUNCT
eurjchem-1602	43	107	,	,	PUNCT
eurjchem-1602	43	108	12.50	12.50	NUM
eurjchem-1602	43	109	(	(	PUNCT
eurjchem-1602	43	110	ch3‐18	ch3‐18	NOUN
eurjchem-1602	43	111	)	)	PUNCT
eurjchem-1602	43	112	,	,	PUNCT
eurjchem-1602	43	113	7.99	7.99	NUM
eurjchem-1602	43	114	(	(	PUNCT
eurjchem-1602	43	115	ch3‐	ch3‐	NOUN
eurjchem-1602	43	116	et	et	PROPN
eurjchem-1602	43	117	)	)	PUNCT
eurjchem-1602	43	118	,	,	PUNCT
eurjchem-1602	43	119	7.60	7.60	NUM
eurjchem-1602	43	120	(	(	PUNCT
eurjchem-1602	43	121	ch3‐et	ch3‐et	NOUN
eurjchem-1602	43	122	)	)	PUNCT
eurjchem-1602	43	123	.	.	PUNCT
eurjchem-1602	44	1	ir	ir	PROPN
eurjchem-1602	44	2	(	(	PUNCT
eurjchem-1602	44	3	nacl	nacl	NOUN
eurjchem-1602	44	4	,	,	PUNCT
eurjchem-1602	44	5	ν	ν	NOUN
eurjchem-1602	44	6	,	,	PUNCT
eurjchem-1602	44	7	cm‐1	cm‐1	PROPN
eurjchem-1602	44	8	):	):	PUNCT
eurjchem-1602	44	9	3491	3491	NUM
eurjchem-1602	44	10	,	,	PUNCT
eurjchem-1602	44	11	3361	3361	NUM
eurjchem-1602	44	12	,	,	PUNCT
eurjchem-1602	44	13	2964	2964	NUM
eurjchem-1602	44	14	,	,	PUNCT
eurjchem-1602	44	15	2879	2879	NUM
eurjchem-1602	44	16	,	,	PUNCT
eurjchem-1602	44	17	2347	2347	NUM
eurjchem-1602	44	18	,	,	PUNCT
eurjchem-1602	44	19	1713	1713	NUM
eurjchem-1602	44	20	,	,	PUNCT
eurjchem-1602	44	21	1460	1460	NUM
eurjchem-1602	44	22	,	,	PUNCT
eurjchem-1602	44	23	1381	1381	NUM
eurjchem-1602	44	24	,	,	PUNCT
eurjchem-1602	44	25	1245	1245	NUM
eurjchem-1602	44	26	,	,	PUNCT
eurjchem-1602	44	27	1145	1145	NUM
eurjchem-1602	44	28	,	,	PUNCT
eurjchem-1602	44	29	958	958	NUM
eurjchem-1602	44	30	,	,	PUNCT
eurjchem-1602	44	31	890	890	NUM
eurjchem-1602	44	32	,	,	PUNCT
eurjchem-1602	44	33	755	755	NUM
eurjchem-1602	44	34	.	.	PUNCT
eurjchem-1602	45	1	ms	ms	NOUN
eurjchem-1602	45	2	(	(	PUNCT
eurjchem-1602	45	3	esi+	esi+	PROPN
eurjchem-1602	45	4	)	)	PUNCT
eurjchem-1602	45	5	(	(	PUNCT
eurjchem-1602	45	6	m	m	PROPN
eurjchem-1602	45	7	/	/	SYM
eurjchem-1602	45	8	z	z	NOUN
eurjchem-1602	45	9	,	,	PUNCT
eurjchem-1602	45	10	(	(	PUNCT
eurjchem-1602	45	11	%	%	INTJ
eurjchem-1602	45	12	)	)	PUNCT
eurjchem-1602	45	13	):	):	PUNCT
eurjchem-1602	45	14	359.25	359.25	NUM
eurjchem-1602	45	15	(	(	PUNCT
eurjchem-1602	45	16	(	(	PUNCT
eurjchem-1602	45	17	m+na)+	m+na)+	PROPN
eurjchem-1602	45	18	,	,	PUNCT
eurjchem-1602	45	19	47	47	NUM
eurjchem-1602	45	20	)	)	PUNCT
eurjchem-1602	45	21	,	,	PUNCT
eurjchem-1602	45	22	319.26	319.26	NUM
eurjchem-1602	45	23	(	(	PUNCT
eurjchem-1602	45	24	(	(	PUNCT
eurjchem-1602	45	25	m‐oh)+	m‐oh)+	X
eurjchem-1602	45	26	,	,	PUNCT
eurjchem-1602	45	27	100	100	NUM
eurjchem-1602	45	28	)	)	PUNCT
eurjchem-1602	45	29	.	.	PUNCT
eurjchem-1602	46	1	hrms	hrm	NOUN
eurjchem-1602	46	2	(	(	PUNCT
eurjchem-1602	46	3	esi+	esi+	ADJ
eurjchem-1602	46	4	):	):	PUNCT
eurjchem-1602	46	5	calculated	calculate	VERB
eurjchem-1602	46	6	for	for	ADP
eurjchem-1602	46	7	c21h36nao3	c21h36nao3	NOUN
eurjchem-1602	46	8	,	,	PUNCT
eurjchem-1602	46	9	359.25567	359.25567	NUM
eurjchem-1602	46	10	g	g	NOUN
eurjchem-1602	46	11	/	/	SYM
eurjchem-1602	46	12	mol	mol	NOUN
eurjchem-1602	46	13	;	;	PUNCT
eurjchem-1602	46	14	found	find	VERB
eurjchem-1602	46	15	:	:	PUNCT
eurjchem-1602	46	16	359.25562	359.25562	NUM
eurjchem-1602	46	17	g	g	NOUN
eurjchem-1602	46	18	/	/	SYM
eurjchem-1602	46	19	mol	mol	NOUN
eurjchem-1602	46	20	.	.	PROPN
eurjchem-1602	47	1	3	3	NUM
eurjchem-1602	47	2	.	.	NOUN
eurjchem-1602	47	3	results	result	NOUN
eurjchem-1602	47	4	and	and	CCONJ
eurjchem-1602	47	5	discussion	discussion	VERB
eurjchem-1602	47	6	the	the	DET
eurjchem-1602	47	7	compound	compound	NOUN
eurjchem-1602	47	8	1	1	NUM
eurjchem-1602	47	9	was	be	AUX
eurjchem-1602	47	10	prepared	prepare	VERB
eurjchem-1602	47	11	by	by	ADP
eurjchem-1602	47	12	a	a	DET
eurjchem-1602	47	13	facile	facile	ADJ
eurjchem-1602	47	14	oxidation	oxidation	NOUN
eurjchem-1602	47	15	of	of	ADP
eurjchem-1602	47	16	compound	compound	NOUN
eurjchem-1602	47	17	2	2	NUM
eurjchem-1602	47	18	with	with	ADP
eurjchem-1602	47	19	pyridinium	pyridinium	NOUN
eurjchem-1602	47	20	dichromate	dichromate	NOUN
eurjchem-1602	47	21	in	in	ADP
eurjchem-1602	47	22	dichloromethane	dichloromethane	NOUN
eurjchem-1602	47	23	(	(	PUNCT
eurjchem-1602	47	24	scheme	scheme	NOUN
eurjchem-1602	47	25	1	1	NUM
eurjchem-1602	47	26	)	)	PUNCT
eurjchem-1602	47	27	.	.	PUNCT
eurjchem-1602	48	1	suitable	suitable	ADJ
eurjchem-1602	48	2	x‐ray	x‐ray	ADJ
eurjchem-1602	48	3	crystals	crystal	NOUN
eurjchem-1602	48	4	diffraction	diffraction	NOUN
eurjchem-1602	48	5	was	be	AUX
eurjchem-1602	48	6	obtained	obtain	VERB
eurjchem-1602	48	7	after	after	ADP
eurjchem-1602	48	8	recrystallization	recrystallization	NOUN
eurjchem-1602	48	9	of	of	ADP
eurjchem-1602	48	10	compound	compound	NOUN
eurjchem-1602	48	11	1	1	NUM
eurjchem-1602	48	12	in	in	ADP
eurjchem-1602	48	13	a	a	DET
eurjchem-1602	48	14	mixture	mixture	NOUN
eurjchem-1602	48	15	of	of	ADP
eurjchem-1602	48	16	hexane	hexane	NOUN
eurjchem-1602	48	17	:	:	PUNCT
eurjchem-1602	48	18	ethyl	ethyl	PROPN
eurjchem-1602	48	19	ether	ether	NOUN
eurjchem-1602	48	20	(	(	PUNCT
eurjchem-1602	48	21	1:1	1:1	NUM
eurjchem-1602	48	22	,	,	PUNCT
eurjchem-1602	48	23	v	v	NOUN
eurjchem-1602	48	24	:	:	PUNCT
eurjchem-1602	48	25	v	v	NOUN
eurjchem-1602	48	26	)	)	PUNCT
eurjchem-1602	48	27	.	.	PUNCT
eurjchem-1602	49	1	the	the	DET
eurjchem-1602	49	2	afforded	afford	VERB
eurjchem-1602	49	3	compound	compound	NOUN
eurjchem-1602	49	4	is	be	AUX
eurjchem-1602	49	5	soluble	soluble	ADJ
eurjchem-1602	49	6	in	in	ADP
eurjchem-1602	49	7	common	common	ADJ
eurjchem-1602	49	8	organic	organic	ADJ
eurjchem-1602	49	9	solvent	solvent	NOUN
eurjchem-1602	49	10	such	such	ADJ
eurjchem-1602	49	11	as	as	ADP
eurjchem-1602	49	12	chloroform	chloroform	NOUN
eurjchem-1602	49	13	.	.	PUNCT
eurjchem-1602	50	1	the	the	DET
eurjchem-1602	50	2	mass	mass	PROPN
eurjchem-1602	50	3	spectrum	spectrum	NOUN
eurjchem-1602	50	4	of	of	ADP
eurjchem-1602	50	5	the	the	DET
eurjchem-1602	50	6	compound	compound	NOUN
eurjchem-1602	50	7	1	1	NUM
eurjchem-1602	50	8	present	present	VERB
eurjchem-1602	50	9	a	a	DET
eurjchem-1602	50	10	peak	peak	NOUN
eurjchem-1602	50	11	at	at	ADP
eurjchem-1602	50	12	359.25562	359.25562	NUM
eurjchem-1602	50	13	amu	amu	NOUN
eurjchem-1602	50	14	corresponding	corresponding	NOUN
eurjchem-1602	50	15	to	to	ADP
eurjchem-1602	50	16	the	the	DET
eurjchem-1602	50	17	molecular	molecular	ADJ
eurjchem-1602	50	18	ion	ion	NOUN
eurjchem-1602	50	19	of	of	ADP
eurjchem-1602	50	20	[	[	X
eurjchem-1602	50	21	1+na]+	1+na]+	NOUN
eurjchem-1602	50	22	.	.	PUNCT
eurjchem-1602	51	1	the	the	DET
eurjchem-1602	51	2	infrared	infrared	PROPN
eurjchem-1602	51	3	spectrum	spectrum	NOUN
eurjchem-1602	51	4	of	of	ADP
eurjchem-1602	51	5	the	the	DET
eurjchem-1602	51	6	compound	compound	NOUN
eurjchem-1602	51	7	shows	show	VERB
eurjchem-1602	51	8	absorption	absorption	NOUN
eurjchem-1602	51	9	band	band	NOUN
eurjchem-1602	51	10	pointed	point	VERB
eurjchem-1602	51	11	at	at	ADP
eurjchem-1602	51	12	1713	1713	NUM
eurjchem-1602	51	13	cm‐1	cm‐1	NOUN
eurjchem-1602	51	14	which	which	PRON
eurjchem-1602	51	15	is	be	AUX
eurjchem-1602	51	16	assigned	assign	VERB
eurjchem-1602	51	17	to	to	ADP
eurjchem-1602	51	18	the	the	DET
eurjchem-1602	51	19	ν(c	ν(c	PROPN
eurjchem-1602	51	20	=	=	SYM
eurjchem-1602	51	21	o	o	NOUN
eurjchem-1602	51	22	)	)	PUNCT
eurjchem-1602	51	23	vibration	vibration	NOUN
eurjchem-1602	51	24	confirming	confirm	VERB
eurjchem-1602	51	25	the	the	DET
eurjchem-1602	51	26	oxidation	oxidation	NOUN
eurjchem-1602	51	27	of	of	ADP
eurjchem-1602	51	28	the	the	DET
eurjchem-1602	51	29	secondary	secondary	ADJ
eurjchem-1602	51	30	alcohol	alcohol	NOUN
eurjchem-1602	51	31	function	function	NOUN
eurjchem-1602	51	32	of	of	ADP
eurjchem-1602	51	33	compound	compound	NOUN
eurjchem-1602	51	34	2	2	NUM
eurjchem-1602	51	35	.	.	PUNCT
eurjchem-1602	52	1	in	in	ADP
eurjchem-1602	52	2	addition	addition	NOUN
eurjchem-1602	52	3	the	the	DET
eurjchem-1602	52	4	13c	13c	NOUN
eurjchem-1602	52	5	nmr	nmr	NOUN
eurjchem-1602	52	6	spectrum	spectrum	NOUN
eurjchem-1602	52	7	recorded	record	VERB
eurjchem-1602	52	8	in	in	ADP
eurjchem-1602	52	9	deuterated	deuterate	VERB
eurjchem-1602	52	10	chloroform	chloroform	NOUN
eurjchem-1602	52	11	shows	show	VERB
eurjchem-1602	52	12	a	a	DET
eurjchem-1602	52	13	characteristic	characteristic	ADJ
eurjchem-1602	52	14	signal	signal	NOUN
eurjchem-1602	52	15	at	at	ADP
eurjchem-1602	52	16	δ	δ	PROPN
eurjchem-1602	52	17	211.91	211.91	NUM
eurjchem-1602	52	18	ppm	ppm	NOUN
eurjchem-1602	52	19	which	which	PRON
eurjchem-1602	52	20	is	be	AUX
eurjchem-1602	52	21	assigned	assign	VERB
eurjchem-1602	52	22	to	to	ADP
eurjchem-1602	52	23	the	the	DET
eurjchem-1602	52	24	c	c	NOUN
eurjchem-1602	52	25	=	=	NOUN
eurjchem-1602	52	26	o.	o.	NOUN
eurjchem-1602	52	27	the	the	DET
eurjchem-1602	52	28	molecular	molecular	ADJ
eurjchem-1602	52	29	structure	structure	NOUN
eurjchem-1602	52	30	of	of	ADP
eurjchem-1602	52	31	the	the	DET
eurjchem-1602	52	32	title	title	NOUN
eurjchem-1602	52	33	compound	compound	NOUN
eurjchem-1602	52	34	is	be	AUX
eurjchem-1602	52	35	shown	show	VERB
eurjchem-1602	52	36	in	in	ADP
eurjchem-1602	52	37	figure	figure	NOUN
eurjchem-1602	52	38	1	1	NUM
eurjchem-1602	52	39	.	.	PUNCT
eurjchem-1602	52	40	crystallographic	crystallographic	ADJ
eurjchem-1602	52	41	data	datum	NOUN
eurjchem-1602	52	42	,	,	PUNCT
eurjchem-1602	52	43	selected	select	VERB
eurjchem-1602	52	44	bond	bond	NOUN
eurjchem-1602	52	45	lengths	length	NOUN
eurjchem-1602	52	46	and	and	CCONJ
eurjchem-1602	52	47	angles	angle	NOUN
eurjchem-1602	52	48	,	,	PUNCT
eurjchem-1602	52	49	hydrogen‐bond	hydrogen‐bond	NOUN
eurjchem-1602	52	50	geometry	geometry	NOUN
eurjchem-1602	52	51	and	and	CCONJ
eurjchem-1602	52	52	atomic	atomic	ADJ
eurjchem-1602	52	53	displacement	displacement	NOUN
eurjchem-1602	52	54	parameters	parameter	NOUN
eurjchem-1602	52	55	are	be	AUX
eurjchem-1602	52	56	listed	list	VERB
eurjchem-1602	52	57	respectively	respectively	ADV
eurjchem-1602	52	58	in	in	ADP
eurjchem-1602	52	59	table	table	NOUN
eurjchem-1602	52	60	1‐4	1‐4	NOUN
eurjchem-1602	52	61	.	.	PUNCT
eurjchem-1602	53	1	the	the	DET
eurjchem-1602	53	2	compound	compound	NOUN
eurjchem-1602	53	3	crystallizes	crystallize	VERB
eurjchem-1602	53	4	in	in	ADP
eurjchem-1602	53	5	the	the	DET
eurjchem-1602	53	6	non‐centrosymmetric	non‐centrosymmetric	PROPN
eurjchem-1602	53	7	space	space	NOUN
eurjchem-1602	53	8	group	group	NOUN
eurjchem-1602	53	9	p21	p21	NOUN
eurjchem-1602	53	10	and	and	CCONJ
eurjchem-1602	53	11	the	the	DET
eurjchem-1602	53	12	absolute	absolute	ADJ
eurjchem-1602	53	13	structure	structure	NOUN
eurjchem-1602	53	14	was	be	AUX
eurjchem-1602	53	15	unambiguously	unambiguously	ADV
eurjchem-1602	53	16	established	establish	VERB
eurjchem-1602	53	17	.	.	PUNCT
eurjchem-1602	54	1	the	the	DET
eurjchem-1602	54	2	molecule	molecule	NOUN
eurjchem-1602	54	3	contains	contain	VERB
eurjchem-1602	54	4	a	a	DET
eurjchem-1602	54	5	cyclopentane	cyclopentane	ADJ
eurjchem-1602	54	6	ring	ring	NOUN
eurjchem-1602	54	7	trans‐fused	trans‐fuse	VERB
eurjchem-1602	54	8	to	to	ADP
eurjchem-1602	54	9	a	a	DET
eurjchem-1602	54	10	cyclohexanone	cyclohexanone	ADJ
eurjchem-1602	54	11	ring	ring	NOUN
eurjchem-1602	54	12	.	.	PUNCT
eurjchem-1602	55	1	the	the	DET
eurjchem-1602	55	2	lateral	lateral	ADJ
eurjchem-1602	55	3	chain	chain	NOUN
eurjchem-1602	55	4	contains	contain	VERB
eurjchem-1602	55	5	an	an	DET
eurjchem-1602	55	6	oxolane	oxolane	NOUN
eurjchem-1602	55	7	ring	ring	NOUN
eurjchem-1602	55	8	.	.	PUNCT
eurjchem-1602	56	1	the	the	DET
eurjchem-1602	56	2	cyclohexanone	cyclohexanone	ADJ
eurjchem-1602	56	3	ring	ring	NOUN
eurjchem-1602	56	4	adopts	adopt	VERB
eurjchem-1602	56	5	a	a	DET
eurjchem-1602	56	6	chair	chair	NOUN
eurjchem-1602	56	7	conformation	conformation	NOUN
eurjchem-1602	56	8	.	.	PUNCT
eurjchem-1602	57	1	the	the	DET
eurjchem-1602	57	2	cyclopentane	cyclopentane	PROPN
eurjchem-1602	57	3	ring	ring	NOUN
eurjchem-1602	57	4	is	be	AUX
eurjchem-1602	57	5	an	an	DET
eurjchem-1602	57	6	envelope	envelope	NOUN
eurjchem-1602	57	7	(	(	PUNCT
eurjchem-1602	57	8	flap	flap	NOUN
eurjchem-1602	57	9	atom	atom	NOUN
eurjchem-1602	57	10	=	=	SYM
eurjchem-1602	57	11	c5	c5	PROPN
eurjchem-1602	57	12	)	)	PUNCT
eurjchem-1602	57	13	and	and	CCONJ
eurjchem-1602	57	14	the	the	DET
eurjchem-1602	57	15	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-1602	57	16	ring	ring	NOUN
eurjchem-1602	57	17	is	be	AUX
eurjchem-1602	57	18	twisted	twist	VERB
eurjchem-1602	57	19	about	about	ADP
eurjchem-1602	57	20	c13‐o2	c13‐o2	PROPN
eurjchem-1602	57	21	.	.	PUNCT
eurjchem-1602	58	1	the	the	DET
eurjchem-1602	58	2	configure‐	configure‐	NOUN
eurjchem-1602	58	3	tions	tion	NOUN
eurjchem-1602	58	4	of	of	ADP
eurjchem-1602	58	5	the	the	DET
eurjchem-1602	58	6	stereogenic	stereogenic	NOUN
eurjchem-1602	58	7	centres	centre	NOUN
eurjchem-1602	58	8	are	be	AUX
eurjchem-1602	58	9	c5(r	c5(r	PROPN
eurjchem-1602	58	10	)	)	PUNCT
eurjchem-1602	58	11	,	,	PUNCT
eurjchem-1602	58	12	c6(r	c6(r	NOUN
eurjchem-1602	58	13	)	)	PUNCT
eurjchem-1602	58	14	,	,	PUNCT
eurjchem-1602	58	15	c9(r	c9(r	PROPN
eurjchem-1602	58	16	)	)	PUNCT
eurjchem-1602	58	17	,	,	PUNCT
eurjchem-1602	58	18	c11(s	c11(s	NOUN
eurjchem-1602	58	19	)	)	PUNCT
eurjchem-1602	58	20	,	,	PUNCT
eurjchem-1602	58	21	c13(r	c13(r	NOUN
eurjchem-1602	58	22	)	)	PUNCT
eurjchem-1602	58	23	and	and	CCONJ
eurjchem-1602	58	24	c16(r	c16(r	NOUN
eurjchem-1602	58	25	)	)	PUNCT
eurjchem-1602	58	26	.	.	PUNCT
eurjchem-1602	59	1	there	there	PRON
eurjchem-1602	59	2	is	be	VERB
eurjchem-1602	59	3	an	an	DET
eurjchem-1602	59	4	intramolecular	intramolecular	ADJ
eurjchem-1602	59	5	o‐h···o	o‐h···o	PROPN
eurjchem-1602	59	6	hydrogen	hydrogen	NOUN
eurjchem-1602	59	7	bond	bond	NOUN
eurjchem-1602	59	8	involving	involve	VERB
eurjchem-1602	59	9	the	the	DET
eurjchem-1602	59	10	hydroxyl	hydroxyl	NOUN
eurjchem-1602	59	11	group	group	NOUN
eurjchem-1602	59	12	(	(	PUNCT
eurjchem-1602	59	13	o3‐h3	o3‐h3	PROPN
eurjchem-1602	59	14	)	)	PUNCT
eurjchem-1602	59	15	and	and	CCONJ
eurjchem-1602	59	16	an	an	DET
eurjchem-1602	59	17	oxolane	oxolane	NOUN
eurjchem-1602	59	18	o	o	NOUN
eurjchem-1602	59	19	atom	atom	NOUN
eurjchem-1602	59	20	(	(	PUNCT
eurjchem-1602	59	21	o2	o2	PROPN
eurjchem-1602	59	22	)	)	PUNCT
eurjchem-1602	59	23	,	,	PUNCT
eurjchem-1602	59	24	generating	generate	VERB
eurjchem-1602	59	25	an	an	DET
eurjchem-1602	59	26	s(5	s(5	PROPN
eurjchem-1602	59	27	)	)	PUNCT
eurjchem-1602	59	28	ring	ring	NOUN
eurjchem-1602	59	29	motif	motif	NOUN
eurjchem-1602	59	30	(	(	PUNCT
eurjchem-1602	59	31	figure	figure	NOUN
eurjchem-1602	59	32	1	1	NUM
eurjchem-1602	59	33	and	and	CCONJ
eurjchem-1602	59	34	table	table	NOUN
eurjchem-1602	59	35	4	4	NUM
eurjchem-1602	59	36	)	)	PUNCT
eurjchem-1602	59	37	.	.	PUNCT
eurjchem-1602	60	1	the	the	DET
eurjchem-1602	60	2	bond	bond	NOUN
eurjchem-1602	60	3	lengths	length	NOUN
eurjchem-1602	60	4	and	and	CCONJ
eurjchem-1602	60	5	angles	angle	NOUN
eurjchem-1602	60	6	are	be	AUX
eurjchem-1602	60	7	normal	normal	ADJ
eurjchem-1602	60	8	and	and	CCONJ
eurjchem-1602	60	9	comparable	comparable	ADJ
eurjchem-1602	60	10	to	to	ADP
eurjchem-1602	60	11	those	those	PRON
eurjchem-1602	60	12	observed	observe	VERB
eurjchem-1602	60	13	in	in	ADP
eurjchem-1602	60	14	compounds	compound	NOUN
eurjchem-1602	60	15	containing	contain	VERB
eurjchem-1602	60	16	the	the	DET
eurjchem-1602	60	17	bicyclic	bicyclic	ADJ
eurjchem-1602	60	18	moiety	moiety	NOUN
eurjchem-1602	60	19	fragment	fragment	NOUN
eurjchem-1602	60	20	(	(	PUNCT
eurjchem-1602	60	21	1s,3ar,7ar)‐1‐ethyl‐7a‐methyl‐	1s,3ar,7ar)‐1‐ethyl‐7a‐methyl‐	NUM
eurjchem-1602	60	22	octahydroinden‐4‐one	octahydroinden‐4‐one	NUM
eurjchem-1602	60	23	)	)	PUNCT
eurjchem-1602	60	24	;	;	PUNCT
eurjchem-1602	60	25	specially	specially	ADV
eurjchem-1602	60	26	in	in	ADP
eurjchem-1602	60	27	our	our	PRON
eurjchem-1602	60	28	recent	recent	ADJ
eurjchem-1602	60	29	work	work	NOUN
eurjchem-1602	60	30	[	[	X
eurjchem-1602	60	31	10	10	NUM
eurjchem-1602	60	32	]	]	PUNCT
eurjchem-1602	60	33	,	,	PUNCT
eurjchem-1602	60	34	which	which	PRON
eurjchem-1602	60	35	concerns	concern	VERB
eurjchem-1602	60	36	an	an	DET
eurjchem-1602	60	37	isomer	isomer	NOUN
eurjchem-1602	60	38	of	of	ADP
eurjchem-1602	60	39	the	the	DET
eurjchem-1602	60	40	title	title	NOUN
eurjchem-1602	60	41	compound	compound	NOUN
eurjchem-1602	60	42	,	,	PUNCT
eurjchem-1602	60	43	adopting	adopt	VERB
eurjchem-1602	60	44	a	a	DET
eurjchem-1602	60	45	very	very	ADV
eurjchem-1602	60	46	similar	similar	ADJ
eurjchem-1602	60	47	crystal	crystal	NOUN
eurjchem-1602	60	48	structure	structure	NOUN
eurjchem-1602	60	49	.	.	PUNCT
eurjchem-1602	61	1	in	in	ADP
eurjchem-1602	61	2	the	the	DET
eurjchem-1602	61	3	crystal	crystal	NOUN
eurjchem-1602	61	4	,	,	PUNCT
eurjchem-1602	61	5	weak	weak	ADJ
eurjchem-1602	61	6	c2‐h2b···o1	c2‐h2b···o1	NOUN
eurjchem-1602	61	7	=	=	SYM
eurjchem-1602	61	8	c	c	NOUN
eurjchem-1602	61	9	hydrogen	hydrogen	NOUN
eurjchem-1602	61	10	bonds	bond	NOUN
eurjchem-1602	61	11	(	(	PUNCT
eurjchem-1602	61	12	table	table	NOUN
eurjchem-1602	61	13	4	4	NUM
eurjchem-1602	61	14	,	,	PUNCT
eurjchem-1602	61	15	figure	figure	NOUN
eurjchem-1602	61	16	2	2	NUM
eurjchem-1602	61	17	)	)	PUNCT
eurjchem-1602	61	18	link	link	VERB
eurjchem-1602	61	19	the	the	DET
eurjchem-1602	61	20	molecules	molecule	NOUN
eurjchem-1602	61	21	into	into	ADP
eurjchem-1602	61	22	c(4	c(4	PROPN
eurjchem-1602	61	23	)	)	PUNCT
eurjchem-1602	61	24	chains	chain	NOUN
eurjchem-1602	61	25	,	,	PUNCT
eurjchem-1602	61	26	which	which	PRON
eurjchem-1602	61	27	propagate	propagate	VERB
eurjchem-1602	61	28	parallel	parallel	NOUN
eurjchem-1602	61	29	to	to	ADP
eurjchem-1602	61	30	[	[	X
eurjchem-1602	61	31	101	101	NUM
eurjchem-1602	61	32	]	]	PUNCT
eurjchem-1602	61	33	.	.	PUNCT
eurjchem-1602	62	1	the	the	DET
eurjchem-1602	62	2	chains	chain	NOUN
eurjchem-1602	62	3	are	be	AUX
eurjchem-1602	62	4	linked	link	VERB
eurjchem-1602	62	5	through	through	ADP
eurjchem-1602	62	6	extremely	extremely	ADV
eurjchem-1602	62	7	weak	weak	ADJ
eurjchem-1602	62	8	hydrogen	hydrogen	NOUN
eurjchem-1602	62	9	bonds	bond	NOUN
eurjchem-1602	62	10	.	.	PUNCT
eurjchem-1602	63	1	comparison	comparison	NOUN
eurjchem-1602	63	2	of	of	ADP
eurjchem-1602	63	3	the	the	DET
eurjchem-1602	63	4	crystal	crystal	NOUN
eurjchem-1602	63	5	structure	structure	NOUN
eurjchem-1602	63	6	with	with	ADP
eurjchem-1602	63	7	that	that	PRON
eurjchem-1602	63	8	of	of	ADP
eurjchem-1602	63	9	the	the	DET
eurjchem-1602	63	10	recent	recent	ADJ
eurjchem-1602	63	11	isomer	isomer	NOUN
eurjchem-1602	63	12	we	we	PRON
eurjchem-1602	63	13	reported	report	VERB
eurjchem-1602	63	14	[	[	X
eurjchem-1602	63	15	10	10	NUM
eurjchem-1602	63	16	]	]	PUNCT
eurjchem-1602	63	17	,	,	PUNCT
eurjchem-1602	63	18	shows	show	VERB
eurjchem-1602	63	19	that	that	SCONJ
eurjchem-1602	63	20	the	the	DET
eurjchem-1602	63	21	two	two	NUM
eurjchem-1602	63	22	isomers	isomer	NOUN
eurjchem-1602	63	23	adopt	adopt	VERB
eurjchem-1602	63	24	similar	similar	ADJ
eurjchem-1602	63	25	supramolecular	supramolecular	ADJ
eurjchem-1602	63	26	architecture	architecture	NOUN
eurjchem-1602	63	27	:	:	PUNCT
eurjchem-1602	63	28	hydrogen	hydrogen	NOUN
eurjchem-1602	63	29	bonds	bond	NOUN
eurjchem-1602	63	30	linking	link	VERB
eurjchem-1602	63	31	molecules	molecule	NOUN
eurjchem-1602	63	32	into	into	ADP
eurjchem-1602	63	33	chains	chain	NOUN
eurjchem-1602	63	34	,	,	PUNCT
eurjchem-1602	63	35	which	which	PRON
eurjchem-1602	63	36	propagate	propagate	VERB
eurjchem-1602	63	37	parallel	parallel	NOUN
eurjchem-1602	63	38	to	to	ADP
eurjchem-1602	63	39	[	[	X
eurjchem-1602	63	40	101	101	NUM
eurjchem-1602	63	41	]	]	PUNCT
eurjchem-1602	63	42	.	.	PUNCT
eurjchem-1602	64	1	in	in	ADP
eurjchem-1602	64	2	both	both	DET
eurjchem-1602	64	3	structures	structure	NOUN
eurjchem-1602	64	4	,	,	PUNCT
eurjchem-1602	64	5	the	the	DET
eurjchem-1602	64	6	chains	chain	NOUN
eurjchem-1602	64	7	are	be	AUX
eurjchem-1602	64	8	linked	link	VERB
eurjchem-1602	64	9	by	by	ADP
eurjchem-1602	64	10	very	very	ADV
eurjchem-1602	64	11	weak	weak	ADJ
eurjchem-1602	64	12	h	h	NOUN
eurjchem-1602	64	13	bonds	bond	NOUN
eurjchem-1602	64	14	.	.	PUNCT
eurjchem-1602	65	1	250	250	NUM
eurjchem-1602	65	2	lo	lo	INTJ
eurjchem-1602	65	3	et	et	PROPN
eurjchem-1602	65	4	al	al	PROPN
eurjchem-1602	65	5	.	.	PUNCT
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eurjchem-1602	65	11	8	8	NUM
eurjchem-1602	65	12	(	(	PUNCT
eurjchem-1602	65	13	3	3	NUM
eurjchem-1602	65	14	)	)	PUNCT
eurjchem-1602	65	15	(	(	PUNCT
eurjchem-1602	65	16	2017	2017	NUM
eurjchem-1602	65	17	)	)	PUNCT
eurjchem-1602	65	18	248‐251	248‐251	NUM
eurjchem-1602	65	19	table	table	NOUN
eurjchem-1602	65	20	1	1	NUM
eurjchem-1602	65	21	.	.	PUNCT
eurjchem-1602	66	1	crystal	crystal	NOUN
eurjchem-1602	66	2	data	datum	NOUN
eurjchem-1602	66	3	and	and	CCONJ
eurjchem-1602	66	4	structure	structure	NOUN
eurjchem-1602	66	5	refinement	refinement	NOUN
eurjchem-1602	66	6	for	for	ADP
eurjchem-1602	66	7	compound	compound	NOUN
eurjchem-1602	66	8	1	1	NUM
eurjchem-1602	66	9	.	.	PUNCT
eurjchem-1602	66	10	empirical	empirical	ADJ
eurjchem-1602	66	11	formula	formula	NOUN
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eurjchem-1602	66	13	formula	formula	VERB
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eurjchem-1602	66	16	temperature	temperature	NOUN
eurjchem-1602	66	17	(	(	PUNCT
eurjchem-1602	66	18	k	k	NOUN
eurjchem-1602	66	19	)	)	PUNCT
eurjchem-1602	66	20	296(2	296(2	NUM
eurjchem-1602	66	21	)	)	PUNCT
eurjchem-1602	66	22	crystal	crystal	NOUN
eurjchem-1602	66	23	shape	shape	NOUN
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eurjchem-1602	66	26	block	block	NOUN
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eurjchem-1602	66	29	crystal	crystal	NOUN
eurjchem-1602	66	30	system	system	NOUN
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eurjchem-1602	66	32	space	space	NOUN
eurjchem-1602	66	33	group	group	NOUN
eurjchem-1602	66	34	p21	p21	PROPN
eurjchem-1602	66	35	a	a	DET
eurjchem-1602	66	36	(	(	PUNCT
eurjchem-1602	66	37	å	å	NOUN
eurjchem-1602	66	38	)	)	PUNCT
eurjchem-1602	66	39	12.4156(19	12.4156(19	NUM
eurjchem-1602	66	40	)	)	PUNCT
eurjchem-1602	66	41	b	b	NOUN
eurjchem-1602	66	42	(	(	PUNCT
eurjchem-1602	66	43	å	å	NOUN
eurjchem-1602	66	44	)	)	PUNCT
eurjchem-1602	66	45	6.3672(6	6.3672(6	NOUN
eurjchem-1602	66	46	)	)	PUNCT
eurjchem-1602	66	47	c	c	NOUN
eurjchem-1602	66	48	(	(	PUNCT
eurjchem-1602	66	49	å	å	NOUN
eurjchem-1602	66	50	)	)	PUNCT
eurjchem-1602	66	51	12.7186(12	12.7186(12	NUM
eurjchem-1602	66	52	)	)	PUNCT
eurjchem-1602	67	1	α	α	PROPN
eurjchem-1602	67	2	(	(	PUNCT
eurjchem-1602	67	3	°	°	PROPN
eurjchem-1602	67	4	)	)	PUNCT
eurjchem-1602	67	5	90	90	NUM
eurjchem-1602	67	6	β	β	X
eurjchem-1602	67	7	(	(	PUNCT
eurjchem-1602	67	8	°	°	NOUN
eurjchem-1602	67	9	)	)	PUNCT
eurjchem-1602	67	10	90.509(5	90.509(5	NOUN
eurjchem-1602	67	11	)	)	PUNCT
eurjchem-1602	67	12	γ	γ	PROPN
eurjchem-1602	67	13	(	(	PUNCT
eurjchem-1602	67	14	°	°	PROPN
eurjchem-1602	67	15	)	)	PUNCT
eurjchem-1602	67	16	90	90	NUM
eurjchem-1602	67	17	volume	volume	NOUN
eurjchem-1602	67	18	(	(	PUNCT
eurjchem-1602	67	19	å3	å3	PROPN
eurjchem-1602	67	20	)	)	PUNCT
eurjchem-1602	67	21	1005.4(2	1005.4(2	NUM
eurjchem-1602	67	22	)	)	PUNCT
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eurjchem-1602	67	24	2	2	NUM
eurjchem-1602	67	25	ρcalc	ρcalc	NOUN
eurjchem-1602	67	26	(	(	PUNCT
eurjchem-1602	67	27	g	g	NOUN
eurjchem-1602	67	28	/	/	SYM
eurjchem-1602	67	29	cm3	cm3	NOUN
eurjchem-1602	67	30	)	)	PUNCT
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eurjchem-1602	67	32	μ	μ	NOUN
eurjchem-1602	67	33	(	(	PUNCT
eurjchem-1602	67	34	mm‐1	mm‐1	PROPN
eurjchem-1602	67	35	)	)	PUNCT
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eurjchem-1602	67	37	f(000	f(000	NOUN
eurjchem-1602	67	38	)	)	PUNCT
eurjchem-1602	67	39	372.0	372.0	NUM
eurjchem-1602	67	40	crystal	crystal	NOUN
eurjchem-1602	67	41	size	size	NOUN
eurjchem-1602	67	42	(	(	PUNCT
eurjchem-1602	67	43	mm3	mm3	PROPN
eurjchem-1602	67	44	)	)	PUNCT
eurjchem-1602	67	45	0.111	0.111	NUM
eurjchem-1602	67	46	×	×	NOUN
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eurjchem-1602	67	48	×	×	NOUN
eurjchem-1602	67	49	0.053	0.053	NUM
eurjchem-1602	67	50	radiation	radiation	NOUN
eurjchem-1602	67	51	cukα	cukα	NOUN
eurjchem-1602	67	52	(	(	PUNCT
eurjchem-1602	67	53	λ	λ	X
eurjchem-1602	67	54	=	=	NOUN
eurjchem-1602	67	55	1.54178	1.54178	NUM
eurjchem-1602	67	56	)	)	PUNCT
eurjchem-1602	67	57	2θ	2θ	NUM
eurjchem-1602	67	58	range	range	VERB
eurjchem-1602	67	59	for	for	ADP
eurjchem-1602	67	60	data	data	NOUN
eurjchem-1602	67	61	collection	collection	NOUN
eurjchem-1602	67	62	(	(	PUNCT
eurjchem-1602	67	63	°	°	PROPN
eurjchem-1602	67	64	)	)	PUNCT
eurjchem-1602	67	65	6.95	6.95	NUM
eurjchem-1602	67	66	to	to	ADP
eurjchem-1602	67	67	143.848	143.848	NUM
eurjchem-1602	67	68	index	index	NOUN
eurjchem-1602	67	69	ranges	range	VERB
eurjchem-1602	67	70	‐15	‐15	VERB
eurjchem-1602	67	71	≤	≤	ADJ
eurjchem-1602	67	72	h	h	NOUN
eurjchem-1602	67	73	≤	≤	NUM
eurjchem-1602	67	74	15	15	NUM
eurjchem-1602	67	75	,	,	PUNCT
eurjchem-1602	67	76	‐7	‐7	PROPN
eurjchem-1602	67	77	≤	≤	PROPN
eurjchem-1602	68	1	k	k	X
eurjchem-1602	68	2	≤	≤	NUM
eurjchem-1602	68	3	7	7	NUM
eurjchem-1602	68	4	,	,	PUNCT
eurjchem-1602	68	5	‐15	‐15	VERB
eurjchem-1602	68	6	≤	≤	NUM
eurjchem-1602	68	7	l	l	NOUN
eurjchem-1602	68	8	≤	≤	NUM
eurjchem-1602	68	9	15	15	NUM
eurjchem-1602	68	10	reflections	reflection	NOUN
eurjchem-1602	68	11	collected	collect	VERB
eurjchem-1602	68	12	12352	12352	NUM
eurjchem-1602	68	13	independent	independent	ADJ
eurjchem-1602	68	14	reflections	reflection	NOUN
eurjchem-1602	68	15	3777	3777	NUM
eurjchem-1602	69	1	[	[	X
eurjchem-1602	69	2	rint	rint	X
eurjchem-1602	69	3	=	=	SYM
eurjchem-1602	69	4	0.0296	0.0296	NUM
eurjchem-1602	69	5	,	,	PUNCT
eurjchem-1602	69	6	rsigma	rsigma	ADJ
eurjchem-1602	69	7	=	=	NOUN
eurjchem-1602	69	8	0.0278	0.0278	NUM
eurjchem-1602	69	9	]	]	PUNCT
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eurjchem-1602	69	11	/	/	SYM
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eurjchem-1602	69	13	/	/	SYM
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eurjchem-1602	69	15	3777/1/221	3777/1/221	NUM
eurjchem-1602	69	16	goodness‐of‐fit	goodness‐of‐fit	PROPN
eurjchem-1602	69	17	on	on	ADP
eurjchem-1602	69	18	f2	f2	PROPN
eurjchem-1602	69	19	1.065	1.065	NUM
eurjchem-1602	69	20	final	final	ADJ
eurjchem-1602	69	21	r	r	NOUN
eurjchem-1602	69	22	indexes	index	NOUN
eurjchem-1602	69	23	[	[	X
eurjchem-1602	69	24	i≥2σ	i≥2σ	X
eurjchem-1602	69	25	(	(	PUNCT
eurjchem-1602	69	26	i	i	NOUN
eurjchem-1602	69	27	)	)	PUNCT
eurjchem-1602	69	28	]	]	PUNCT
eurjchem-1602	70	1	r1	r1	PROPN
eurjchem-1602	70	2	=	=	SYM
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eurjchem-1602	70	4	,	,	PUNCT
eurjchem-1602	70	5	wr2	wr2	PROPN
eurjchem-1602	70	6	=	=	PROPN
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eurjchem-1602	70	9	r	r	NOUN
eurjchem-1602	70	10	indexes	index	NOUN
eurjchem-1602	70	11	[	[	X
eurjchem-1602	70	12	all	all	DET
eurjchem-1602	70	13	data	datum	NOUN
eurjchem-1602	70	14	]	]	PUNCT
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eurjchem-1602	70	16	=	=	PUNCT
eurjchem-1602	70	17	0.0384	0.0384	PROPN
eurjchem-1602	70	18	,	,	PUNCT
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eurjchem-1602	70	20	=	=	PROPN
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eurjchem-1602	70	24	.	.	PUNCT
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eurjchem-1602	70	28	(	(	PUNCT
eurjchem-1602	70	29	e	e	NOUN
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eurjchem-1602	71	15	length	length	NOUN
eurjchem-1602	71	16	(	(	PUNCT
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eurjchem-1602	71	18	)	)	PUNCT
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eurjchem-1602	71	20	c1	c1	NOUN
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eurjchem-1602	71	24	c8	c8	PROPN
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eurjchem-1602	71	36	c13	c13	PROPN
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eurjchem-1602	71	48	c12	c12	PROPN
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eurjchem-1602	71	69	1.519(4	1.519(4	PROPN
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eurjchem-1602	71	72	c15	c15	PROPN
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eurjchem-1602	71	84	c5	c5	PROPN
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eurjchem-1602	71	88	c17	c17	NOUN
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eurjchem-1602	71	90	)	)	PUNCT
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eurjchem-1602	72	2	c10	c10	VERB
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eurjchem-1602	72	6	c20	c20	PROPN
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eurjchem-1602	72	10	c9	c9	PROPN
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eurjchem-1602	72	14	c18	c18	NOUN
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eurjchem-1602	72	18	c6	c6	PROPN
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eurjchem-1602	72	20	)	)	PUNCT
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eurjchem-1602	72	22	c19	c19	PROPN
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eurjchem-1602	72	24	)	)	PUNCT
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eurjchem-1602	72	26	c7	c7	PROPN
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eurjchem-1602	72	28	)	)	PUNCT
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eurjchem-1602	72	30	c21	c21	NOUN
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eurjchem-1602	72	32	)	)	PUNCT
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eurjchem-1602	72	34	3	3	NUM
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eurjchem-1602	72	40	1	1	NUM
eurjchem-1602	72	41	.	.	PUNCT
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eurjchem-1602	72	44	atom	atom	NOUN
eurjchem-1602	72	45	angle	angle	NOUN
eurjchem-1602	72	46	(	(	PUNCT
eurjchem-1602	72	47	°	°	NOUN
eurjchem-1602	72	48	)	)	PUNCT
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eurjchem-1602	72	50	atom	atom	NOUN
eurjchem-1602	72	51	atom	atom	NOUN
eurjchem-1602	72	52	angle	angle	NOUN
eurjchem-1602	72	53	(	(	PUNCT
eurjchem-1602	72	54	°	°	PROPN
eurjchem-1602	72	55	)	)	PUNCT
eurjchem-1602	72	56	c16	c16	PROPN
eurjchem-1602	72	57	o2	o2	PROPN
eurjchem-1602	72	58	c13	c13	PROPN
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eurjchem-1602	72	60	)	)	PUNCT
eurjchem-1602	73	1	c5	c5	PROPN
eurjchem-1602	73	2	c9	c9	PROPN
eurjchem-1602	73	3	c8	c8	PROPN
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eurjchem-1602	73	5	)	)	PUNCT
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eurjchem-1602	73	7	c1	c1	PROPN
eurjchem-1602	73	8	c6	c6	PROPN
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eurjchem-1602	73	10	)	)	PUNCT
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eurjchem-1602	73	13	c9	c9	NOUN
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eurjchem-1602	73	15	)	)	PUNCT
eurjchem-1602	73	16	o1	o1	NOUN
eurjchem-1602	73	17	c1	c1	NOUN
eurjchem-1602	73	18	c2	c2	PROPN
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eurjchem-1602	73	20	)	)	PUNCT
eurjchem-1602	73	21	c12	c12	PROPN
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eurjchem-1602	73	23	c13	c13	PROPN
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eurjchem-1602	73	25	)	)	PUNCT
eurjchem-1602	74	1	c6	c6	PROPN
eurjchem-1602	74	2	c1	c1	PROPN
eurjchem-1602	74	3	c2	c2	PROPN
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eurjchem-1602	74	5	)	)	PUNCT
eurjchem-1602	74	6	c9	c9	PROPN
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eurjchem-1602	74	8	c13	c13	PROPN
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eurjchem-1602	74	11	c1	c1	PROPN
eurjchem-1602	74	12	c2	c2	PROPN
eurjchem-1602	74	13	c3	c3	PROPN
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eurjchem-1602	74	16	o2	o2	PROPN
eurjchem-1602	74	17	c13	c13	PROPN
eurjchem-1602	74	18	c14	c14	PROPN
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eurjchem-1602	74	20	)	)	PUNCT
eurjchem-1602	74	21	c2	c2	PROPN
eurjchem-1602	74	22	c3	c3	PROPN
eurjchem-1602	74	23	c4	c4	PROPN
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eurjchem-1602	74	25	)	)	PUNCT
eurjchem-1602	74	26	o2	o2	PROPN
eurjchem-1602	74	27	c13	c13	PROPN
eurjchem-1602	74	28	c11	c11	NOUN
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eurjchem-1602	74	30	)	)	PUNCT
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eurjchem-1602	74	32	c4	c4	PROPN
eurjchem-1602	74	33	c5	c5	PROPN
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eurjchem-1602	74	37	c13	c13	PROPN
eurjchem-1602	74	38	c11	c11	PROPN
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eurjchem-1602	74	41	c4	c4	PROPN
eurjchem-1602	74	42	c5	c5	PROPN
eurjchem-1602	74	43	c10	c10	VERB
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eurjchem-1602	74	45	)	)	PUNCT
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eurjchem-1602	74	47	c14	c14	PROPN
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eurjchem-1602	74	50	)	)	PUNCT
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eurjchem-1602	74	52	c5	c5	PROPN
eurjchem-1602	74	53	c9	c9	PROPN
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eurjchem-1602	74	57	c15	c15	PROPN
eurjchem-1602	74	58	c14	c14	PROPN
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eurjchem-1602	74	62	c5	c5	PROPN
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eurjchem-1602	75	3	c15	c15	PROPN
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eurjchem-1602	75	5	)	)	PUNCT
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eurjchem-1602	75	7	c5	c5	PROPN
eurjchem-1602	75	8	c6	c6	PROPN
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eurjchem-1602	75	12	c16	c16	PROPN
eurjchem-1602	75	13	c17	c17	PROPN
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eurjchem-1602	75	17	c5	c5	PROPN
eurjchem-1602	75	18	c6	c6	PROPN
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eurjchem-1602	75	22	c16	c16	PROPN
eurjchem-1602	75	23	c17	c17	PROPN
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eurjchem-1602	76	3	c7	c7	PROPN
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eurjchem-1602	77	3	c5	c5	PROPN
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eurjchem-1602	78	3	c5	c5	PROPN
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eurjchem-1602	79	3	c8	c8	PROPN
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eurjchem-1602	80	3	c9	c9	PROPN
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eurjchem-1602	80	8	c18	c18	PROPN
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eurjchem-1602	80	13	c5	c5	PROPN
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eurjchem-1602	80	18	c17	c17	PROPN
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eurjchem-1602	80	20	)	)	PUNCT
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eurjchem-1602	80	23	c8	c8	PROPN
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eurjchem-1602	80	25	)	)	PUNCT
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eurjchem-1602	80	28	c17	c17	PROPN
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eurjchem-1602	80	30	)	)	PUNCT
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eurjchem-1602	80	32	title	title	NOUN
eurjchem-1602	80	33	isomer	isomer	NOUN
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eurjchem-1602	80	37	the	the	DET
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eurjchem-1602	80	40	an	an	DET
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eurjchem-1602	80	42	hydrogen	hydrogen	NOUN
eurjchem-1602	80	43	bond	bond	NOUN
eurjchem-1602	80	44	and	and	CCONJ
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eurjchem-1602	80	47	in	in	ADP
eurjchem-1602	80	48	the	the	DET
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eurjchem-1602	80	50	are	be	AUX
eurjchem-1602	80	51	linked	link	VERB
eurjchem-1602	80	52	by	by	ADP
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eurjchem-1602	80	54	h	h	NOUN
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eurjchem-1602	80	56	.	.	PUNCT
eurjchem-1602	81	1	on	on	ADP
eurjchem-1602	81	2	the	the	DET
eurjchem-1602	81	3	contrary	contrary	NOUN
eurjchem-1602	81	4	,	,	PUNCT
eurjchem-1602	81	5	in	in	ADP
eurjchem-1602	81	6	the	the	DET
eurjchem-1602	81	7	previously	previously	ADV
eurjchem-1602	81	8	reported	report	VERB
eurjchem-1602	81	9	isomer	isomer	PROPN
eurjchem-1602	81	10	,	,	PUNCT
eurjchem-1602	81	11	there	there	PRON
eurjchem-1602	81	12	is	be	VERB
eurjchem-1602	81	13	no	no	DET
eurjchem-1602	81	14	intramolecular	intramolecular	ADJ
eurjchem-1602	81	15	h	h	NOUN
eurjchem-1602	81	16	bond	bond	NOUN
eurjchem-1602	81	17	and	and	CCONJ
eurjchem-1602	81	18	the	the	DET
eurjchem-1602	81	19	molecules	molecule	NOUN
eurjchem-1602	81	20	in	in	ADP
eurjchem-1602	81	21	the	the	DET
eurjchem-1602	81	22	chains	chain	NOUN
eurjchem-1602	81	23	are	be	AUX
eurjchem-1602	81	24	strongly	strongly	ADV
eurjchem-1602	81	25	linked	link	VERB
eurjchem-1602	81	26	.	.	PUNCT
eurjchem-1602	82	1	it	it	PRON
eurjchem-1602	82	2	should	should	AUX
eurjchem-1602	82	3	be	be	AUX
eurjchem-1602	82	4	mentioned	mention	VERB
eurjchem-1602	82	5	that	that	SCONJ
eurjchem-1602	82	6	the	the	DET
eurjchem-1602	82	7	crystal	crystal	NOUN
eurjchem-1602	82	8	structure	structure	NOUN
eurjchem-1602	82	9	change	change	NOUN
eurjchem-1602	82	10	between	between	ADP
eurjchem-1602	82	11	the	the	DET
eurjchem-1602	82	12	two	two	NUM
eurjchem-1602	82	13	isomers	isomer	NOUN
eurjchem-1602	82	14	affected	affect	VERB
eurjchem-1602	82	15	mainly	mainly	ADV
eurjchem-1602	82	16	the	the	DET
eurjchem-1602	82	17	unit	unit	NOUN
eurjchem-1602	82	18	cell	cell	NOUN
eurjchem-1602	82	19	lattice	lattice	PROPN
eurjchem-1602	82	20	,	,	PUNCT
eurjchem-1602	82	21	but	but	CCONJ
eurjchem-1602	82	22	not	not	PART
eurjchem-1602	82	23	the	the	DET
eurjchem-1602	82	24	crystal	crystal	NOUN
eurjchem-1602	82	25	system	system	NOUN
eurjchem-1602	82	26	(	(	PUNCT
eurjchem-1602	82	27	monoclinic	monoclinic	ADJ
eurjchem-1602	82	28	)	)	PUNCT
eurjchem-1602	82	29	,	,	PUNCT
eurjchem-1602	82	30	nor	nor	CCONJ
eurjchem-1602	82	31	the	the	DET
eurjchem-1602	82	32	space	space	NOUN
eurjchem-1602	82	33	group	group	NOUN
eurjchem-1602	82	34	symmetry	symmetry	NOUN
eurjchem-1602	82	35	(	(	PUNCT
eurjchem-1602	82	36	p21	p21	PROPN
eurjchem-1602	82	37	)	)	PUNCT
eurjchem-1602	82	38	.	.	PUNCT
eurjchem-1602	83	1	indeed	indeed	ADV
eurjchem-1602	83	2	,	,	PUNCT
eurjchem-1602	83	3	the	the	DET
eurjchem-1602	83	4	unit	unit	NOUN
eurjchem-1602	83	5	cell	cell	NOUN
eurjchem-1602	83	6	volume	volume	NOUN
eurjchem-1602	83	7	expands	expand	VERB
eurjchem-1602	83	8	from	from	ADP
eurjchem-1602	83	9	the	the	DET
eurjchem-1602	83	10	precedent	precedent	NOUN
eurjchem-1602	83	11	isomer	isomer	ADJ
eurjchem-1602	83	12	to	to	ADP
eurjchem-1602	83	13	the	the	DET
eurjchem-1602	83	14	title	title	NOUN
eurjchem-1602	83	15	isomer	isomer	NOUN
eurjchem-1602	83	16	(	(	PUNCT
eurjchem-1602	83	17	979.3	979.3	NUM
eurjchem-1602	83	18	to	to	ADP
eurjchem-1602	83	19	1005.3	1005.3	NUM
eurjchem-1602	83	20	å3	å3	PROPN
eurjchem-1602	83	21	)	)	PUNCT
eurjchem-1602	83	22	.	.	PUNCT
eurjchem-1602	84	1	this	this	DET
eurjchem-1602	84	2	expansion	expansion	NOUN
eurjchem-1602	84	3	resulted	result	VERB
eurjchem-1602	84	4	from	from	ADP
eurjchem-1602	84	5	contraction	contraction	NOUN
eurjchem-1602	84	6	in	in	ADP
eurjchem-1602	84	7	the	the	DET
eurjchem-1602	84	8	c	c	PROPN
eurjchem-1602	84	9	parameter	parameter	NOUN
eurjchem-1602	84	10	and	and	CCONJ
eurjchem-1602	84	11	the	the	DET
eurjchem-1602	84	12	increase	increase	NOUN
eurjchem-1602	84	13	of	of	ADP
eurjchem-1602	84	14	the	the	DET
eurjchem-1602	84	15	a	a	DET
eurjchem-1602	84	16	parameter	parameter	NOUN
eurjchem-1602	84	17	,	,	PUNCT
eurjchem-1602	84	18	so	so	SCONJ
eurjchem-1602	84	19	that	that	SCONJ
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eurjchem-1602	84	21	c	c	NOUN
eurjchem-1602	84	22	/	/	SYM
eurjchem-1602	84	23	a	a	DET
eurjchem-1602	84	24	ratio	ratio	NOUN
eurjchem-1602	84	25	and	and	CCONJ
eurjchem-1602	84	26	the	the	DET
eurjchem-1602	84	27	β	β	PROPN
eurjchem-1602	84	28	angle	angle	NOUN
eurjchem-1602	84	29	decreased	decrease	VERB
eurjchem-1602	84	30	from	from	ADP
eurjchem-1602	84	31	1.8	1.8	NUM
eurjchem-1602	84	32	°	°	NOUN
eurjchem-1602	84	33	to	to	ADP
eurjchem-1602	84	34	1.0	1.0	NUM
eurjchem-1602	84	35	°	°	NOUN
eurjchem-1602	84	36	and	and	CCONJ
eurjchem-1602	84	37	104.2	104.2	NUM
eurjchem-1602	84	38	to	to	PART
eurjchem-1602	84	39	90.5	90.5	NUM
eurjchem-1602	84	40	°	°	NOUN
eurjchem-1602	84	41	,	,	PUNCT
eurjchem-1602	84	42	respectively	respectively	ADV
eurjchem-1602	84	43	.	.	PUNCT
eurjchem-1602	85	1	the	the	DET
eurjchem-1602	85	2	b	b	PROPN
eurjchem-1602	85	3	parameter	parameter	NOUN
eurjchem-1602	85	4	remains	remain	VERB
eurjchem-1602	85	5	almost	almost	ADV
eurjchem-1602	85	6	unchanged	unchanged	ADJ
eurjchem-1602	85	7	.	.	PUNCT
eurjchem-1602	86	1	4	4	X
eurjchem-1602	86	2	.	.	X
eurjchem-1602	86	3	conclusion	conclusion	VERB
eurjchem-1602	86	4	the	the	DET
eurjchem-1602	86	5	titled	title	VERB
eurjchem-1602	86	6	compound	compound	NOUN
eurjchem-1602	86	7	having	have	VERB
eurjchem-1602	86	8	an	an	DET
eurjchem-1602	86	9	oxolane	oxolane	NOUN
eurjchem-1602	86	10	moiety	moiety	NOUN
eurjchem-1602	86	11	in	in	ADP
eurjchem-1602	86	12	his	his	PRON
eurjchem-1602	86	13	side	side	NOUN
eurjchem-1602	86	14	chain	chain	NOUN
eurjchem-1602	86	15	was	be	AUX
eurjchem-1602	86	16	synthesized	synthesize	VERB
eurjchem-1602	86	17	successfully	successfully	ADV
eurjchem-1602	86	18	and	and	CCONJ
eurjchem-1602	86	19	its	its	PRON
eurjchem-1602	86	20	structure	structure	NOUN
eurjchem-1602	86	21	has	have	AUX
eurjchem-1602	86	22	been	be	AUX
eurjchem-1602	86	23	determined	determine	VERB
eurjchem-1602	86	24	by	by	ADP
eurjchem-1602	86	25	x‐ray	x‐ray	ADJ
eurjchem-1602	86	26	single	single	ADJ
eurjchem-1602	86	27	crystallography	crystallography	NOUN
eurjchem-1602	86	28	.	.	PUNCT
eurjchem-1602	87	1	one	one	NUM
eurjchem-1602	87	2	of	of	ADP
eurjchem-1602	87	3	his	his	PRON
eurjchem-1602	87	4	stereo‐	stereo‐	NOUN
eurjchem-1602	87	5	isomer	isomer	PROPN
eurjchem-1602	87	6	was	be	AUX
eurjchem-1602	87	7	previously	previously	ADV
eurjchem-1602	87	8	synthetized	synthetize	VERB
eurjchem-1602	87	9	and	and	CCONJ
eurjchem-1602	87	10	reported	report	VERB
eurjchem-1602	87	11	by	by	ADP
eurjchem-1602	87	12	our	our	PRON
eurjchem-1602	87	13	group	group	NOUN
eurjchem-1602	87	14	.	.	PUNCT
eurjchem-1602	88	1	lo	lo	PROPN
eurjchem-1602	88	2	et	et	PROPN
eurjchem-1602	88	3	al	al	PROPN
eurjchem-1602	88	4	.	.	PUNCT
eurjchem-1602	88	5	/	/	SYM
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eurjchem-1602	88	9	chemistry	chemistry	NOUN
eurjchem-1602	88	10	8	8	NUM
eurjchem-1602	88	11	(	(	PUNCT
eurjchem-1602	88	12	3	3	NUM
eurjchem-1602	88	13	)	)	PUNCT
eurjchem-1602	88	14	(	(	PUNCT
eurjchem-1602	88	15	2017	2017	NUM
eurjchem-1602	88	16	)	)	PUNCT
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eurjchem-1602	88	18	251	251	NUM
eurjchem-1602	88	19	table	table	NOUN
eurjchem-1602	88	20	4	4	NUM
eurjchem-1602	88	21	.	.	PUNCT
eurjchem-1602	88	22	anisotropic	anisotropic	NOUN
eurjchem-1602	88	23	displacement	displacement	ADJ
eurjchem-1602	88	24	parameters	parameter	NOUN
eurjchem-1602	88	25	(	(	PUNCT
eurjchem-1602	88	26	å2×103	å2×103	NOUN
eurjchem-1602	88	27	)	)	PUNCT
eurjchem-1602	88	28	for	for	ADP
eurjchem-1602	88	29	compound	compound	NOUN
eurjchem-1602	88	30	1	1	NUM
eurjchem-1602	88	31	.	.	PUNCT
eurjchem-1602	89	1	the	the	DET
eurjchem-1602	89	2	anisotropic	anisotropic	NOUN
eurjchem-1602	89	3	displacement	displacement	NOUN
eurjchem-1602	89	4	factor	factor	NOUN
eurjchem-1602	89	5	exponent	exponent	NOUN
eurjchem-1602	89	6	takes	take	VERB
eurjchem-1602	89	7	the	the	DET
eurjchem-1602	89	8	form	form	NOUN
eurjchem-1602	89	9	:	:	PUNCT
eurjchem-1602	89	10	‐2π2[h2a*2u11	‐2π2[h2a*2u11	X
eurjchem-1602	89	11	+	+	PROPN
eurjchem-1602	89	12	2hka*b*u12	2hka*b*u12	NUM
eurjchem-1602	89	13	+	+	NOUN
eurjchem-1602	89	14	…	…	PUNCT
eurjchem-1602	89	15	]	]	X
eurjchem-1602	89	16	.	.	PUNCT
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eurjchem-1602	90	2	u11	u11	PROPN
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eurjchem-1602	90	4	u33	u33	PROPN
eurjchem-1602	90	5	u23	u23	PROPN
eurjchem-1602	90	6	u13	u13	PROPN
eurjchem-1602	90	7	u12	u12	PROPN
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eurjchem-1602	90	9	84.8(11	84.8(11	NUM
eurjchem-1602	90	10	)	)	PUNCT
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eurjchem-1602	90	12	)	)	PUNCT
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eurjchem-1602	90	14	)	)	PUNCT
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eurjchem-1602	90	16	)	)	PUNCT
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eurjchem-1602	90	18	)	)	PUNCT
eurjchem-1602	90	19	‐0.2(9	‐0.2(9	NUM
eurjchem-1602	90	20	)	)	PUNCT
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eurjchem-1602	90	25	)	)	PUNCT
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eurjchem-1602	90	27	)	)	PUNCT
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eurjchem-1602	90	29	)	)	PUNCT
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eurjchem-1602	90	31	)	)	PUNCT
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eurjchem-1602	90	33	)	)	PUNCT
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eurjchem-1602	90	36	)	)	PUNCT
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eurjchem-1602	90	40	)	)	PUNCT
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eurjchem-1602	90	42	)	)	PUNCT
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eurjchem-1602	90	46	)	)	PUNCT
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eurjchem-1602	90	49	)	)	PUNCT
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eurjchem-1602	90	51	)	)	PUNCT
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eurjchem-1602	90	53	)	)	PUNCT
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eurjchem-1602	90	55	)	)	PUNCT
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eurjchem-1602	90	57	)	)	PUNCT
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eurjchem-1602	90	59	)	)	PUNCT
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eurjchem-1602	90	62	)	)	PUNCT
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eurjchem-1602	90	64	)	)	PUNCT
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eurjchem-1602	90	66	)	)	PUNCT
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eurjchem-1602	90	68	)	)	PUNCT
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eurjchem-1602	90	70	)	)	PUNCT
eurjchem-1602	90	71	‐3.9(11	‐3.9(11	NOUN
eurjchem-1602	90	72	)	)	PUNCT
eurjchem-1602	90	73	c3	c3	PROPN
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eurjchem-1602	90	75	)	)	PUNCT
eurjchem-1602	90	76	77.9(16	77.9(16	NUM
eurjchem-1602	90	77	)	)	PUNCT
eurjchem-1602	90	78	90.0(17	90.0(17	NUM
eurjchem-1602	90	79	)	)	PUNCT
eurjchem-1602	90	80	‐3.0(14	‐3.0(14	NOUN
eurjchem-1602	90	81	)	)	PUNCT
eurjchem-1602	90	82	3.0(11	3.0(11	NOUN
eurjchem-1602	90	83	)	)	PUNCT
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eurjchem-1602	90	85	)	)	PUNCT
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eurjchem-1602	90	87	53.3(11	53.3(11	NUM
eurjchem-1602	90	88	)	)	PUNCT
eurjchem-1602	90	89	69.7(14	69.7(14	NUM
eurjchem-1602	90	90	)	)	PUNCT
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eurjchem-1602	90	92	)	)	PUNCT
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eurjchem-1602	90	94	)	)	PUNCT
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eurjchem-1602	90	96	)	)	PUNCT
eurjchem-1602	90	97	‐7.1(11	‐7.1(11	NUM
eurjchem-1602	90	98	)	)	PUNCT
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eurjchem-1602	90	101	)	)	PUNCT
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eurjchem-1602	90	103	)	)	PUNCT
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eurjchem-1602	90	105	)	)	PUNCT
eurjchem-1602	90	106	1.5(9	1.5(9	NUM
eurjchem-1602	90	107	)	)	PUNCT
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eurjchem-1602	90	109	)	)	PUNCT
eurjchem-1602	90	110	‐1.7(9	‐1.7(9	NUM
eurjchem-1602	90	111	)	)	PUNCT
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eurjchem-1602	90	114	)	)	PUNCT
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eurjchem-1602	90	116	)	)	PUNCT
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eurjchem-1602	90	118	)	)	PUNCT
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eurjchem-1602	90	120	)	)	PUNCT
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eurjchem-1602	90	122	)	)	PUNCT
eurjchem-1602	90	123	‐1.2(9	‐1.2(9	NUM
eurjchem-1602	90	124	)	)	PUNCT
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eurjchem-1602	90	126	55.7(12	55.7(12	NUM
eurjchem-1602	90	127	)	)	PUNCT
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eurjchem-1602	90	129	)	)	PUNCT
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eurjchem-1602	90	131	)	)	PUNCT
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eurjchem-1602	90	133	)	)	PUNCT
eurjchem-1602	90	134	0.9(9	0.9(9	NOUN
eurjchem-1602	90	135	)	)	PUNCT
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eurjchem-1602	90	137	)	)	PUNCT
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eurjchem-1602	90	140	)	)	PUNCT
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eurjchem-1602	90	142	)	)	PUNCT
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eurjchem-1602	90	144	)	)	PUNCT
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eurjchem-1602	90	146	)	)	PUNCT
eurjchem-1602	90	147	1.9(8	1.9(8	NUM
eurjchem-1602	90	148	)	)	PUNCT
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eurjchem-1602	90	150	)	)	PUNCT
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eurjchem-1602	90	152	49.4(10	49.4(10	NUM
eurjchem-1602	90	153	)	)	PUNCT
eurjchem-1602	90	154	43.7(10	43.7(10	NOUN
eurjchem-1602	90	155	)	)	PUNCT
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eurjchem-1602	90	157	)	)	PUNCT
eurjchem-1602	90	158	1.9(8	1.9(8	NUM
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eurjchem-1602	90	166	)	)	PUNCT
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eurjchem-1602	90	168	)	)	PUNCT
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eurjchem-1602	90	170	)	)	PUNCT
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eurjchem-1602	90	172	)	)	PUNCT
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eurjchem-1602	91	2	)	)	PUNCT
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eurjchem-1602	91	8	)	)	PUNCT
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eurjchem-1602	91	10	)	)	PUNCT
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eurjchem-1602	91	17	)	)	PUNCT
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eurjchem-1602	91	23	)	)	PUNCT
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eurjchem-1602	93	14	7.5(8	7.5(8	NUM
eurjchem-1602	93	15	)	)	PUNCT
eurjchem-1602	93	16	‐1.9(8	‐1.9(8	NUM
eurjchem-1602	93	17	)	)	PUNCT
eurjchem-1602	93	18	‐1.2(8	‐1.2(8	X
eurjchem-1602	93	19	)	)	PUNCT
eurjchem-1602	93	20	c17	c17	NOUN
eurjchem-1602	93	21	50.7(10	50.7(10	NUM
eurjchem-1602	93	22	)	)	PUNCT
eurjchem-1602	93	23	52.7(11	52.7(11	NUM
eurjchem-1602	93	24	)	)	PUNCT
eurjchem-1602	93	25	53.2(10	53.2(10	NOUN
eurjchem-1602	93	26	)	)	PUNCT
eurjchem-1602	93	27	5.7(9	5.7(9	NUM
eurjchem-1602	93	28	)	)	PUNCT
eurjchem-1602	93	29	‐2.6(8	‐2.6(8	NUM
eurjchem-1602	93	30	)	)	PUNCT
eurjchem-1602	93	31	‐4.3(9	‐4.3(9	NUM
eurjchem-1602	93	32	)	)	PUNCT
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eurjchem-1602	93	34	63.8(12	63.8(12	NUM
eurjchem-1602	93	35	)	)	PUNCT
eurjchem-1602	93	36	52.2(11	52.2(11	NUM
eurjchem-1602	93	37	)	)	PUNCT
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eurjchem-1602	93	39	)	)	PUNCT
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eurjchem-1602	93	41	)	)	PUNCT
eurjchem-1602	93	42	8(1	8(1	NOUN
eurjchem-1602	93	43	)	)	PUNCT
eurjchem-1602	93	44	2.4(10	2.4(10	NUM
eurjchem-1602	93	45	)	)	PUNCT
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eurjchem-1602	93	47	81.3(17	81.3(17	NUM
eurjchem-1602	93	48	)	)	PUNCT
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eurjchem-1602	93	50	)	)	PUNCT
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eurjchem-1602	93	52	)	)	PUNCT
eurjchem-1602	93	53	‐22.7(15	‐22.7(15	NOUN
eurjchem-1602	93	54	)	)	PUNCT
eurjchem-1602	93	55	‐2.2(14	‐2.2(14	NOUN
eurjchem-1602	93	56	)	)	PUNCT
eurjchem-1602	93	57	‐9.7(14	‐9.7(14	NOUN
eurjchem-1602	93	58	)	)	PUNCT
eurjchem-1602	93	59	c20	c20	NOUN
eurjchem-1602	93	60	82.4(16	82.4(16	NOUN
eurjchem-1602	93	61	)	)	PUNCT
eurjchem-1602	93	62	56.4(13	56.4(13	NUM
eurjchem-1602	93	63	)	)	PUNCT
eurjchem-1602	93	64	64.6(13	64.6(13	NUM
eurjchem-1602	93	65	)	)	PUNCT
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eurjchem-1602	93	67	)	)	PUNCT
eurjchem-1602	93	68	5.7(12	5.7(12	NOUN
eurjchem-1602	93	69	)	)	PUNCT
eurjchem-1602	93	70	‐12.0(12	‐12.0(12	NUM
eurjchem-1602	93	71	)	)	PUNCT
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eurjchem-1602	93	74	)	)	PUNCT
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eurjchem-1602	93	76	)	)	PUNCT
eurjchem-1602	93	77	71.2(16	71.2(16	NOUN
eurjchem-1602	93	78	)	)	PUNCT
eurjchem-1602	93	79	7.6(16	7.6(16	NOUN
eurjchem-1602	93	80	)	)	PUNCT
eurjchem-1602	93	81	25.6(16	25.6(16	NUM
eurjchem-1602	93	82	)	)	PUNCT
eurjchem-1602	93	83	‐26.4(19	‐26.4(19	NUM
eurjchem-1602	93	84	)	)	PUNCT
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eurjchem-1602	93	86	5	5	NUM
eurjchem-1602	93	87	.	.	PUNCT
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eurjchem-1602	94	4	compound	compound	NOUN
eurjchem-1602	94	5	1	1	NUM
eurjchem-1602	94	6	.	.	PUNCT
eurjchem-1602	95	1	d	d	NOUN
eurjchem-1602	95	2	h	h	NOUN
eurjchem-1602	95	3	a	a	DET
eurjchem-1602	95	4	d(d‐h	d(d‐h	PROPN
eurjchem-1602	95	5	)	)	PUNCT
eurjchem-1602	95	6	(	(	PUNCT
eurjchem-1602	95	7	å	å	X
eurjchem-1602	95	8	)	)	PUNCT
eurjchem-1602	95	9	d(h‐a	d(h‐a	PROPN
eurjchem-1602	95	10	)	)	PUNCT
eurjchem-1602	96	1	(	(	PUNCT
eurjchem-1602	96	2	å	å	X
eurjchem-1602	96	3	)	)	PUNCT
eurjchem-1602	96	4	d(d‐a	d(d‐a	NUM
eurjchem-1602	96	5	)	)	PUNCT
eurjchem-1602	96	6	(	(	PUNCT
eurjchem-1602	96	7	å	å	NOUN
eurjchem-1602	96	8	)	)	PUNCT
eurjchem-1602	96	9	d‐h‐a	d‐h‐a	NOUN
eurjchem-1602	96	10	(	(	PUNCT
eurjchem-1602	96	11	°	°	PROPN
eurjchem-1602	96	12	)	)	PUNCT
eurjchem-1602	96	13	o3	o3	PROPN
eurjchem-1602	96	14	h3	h3	PROPN
eurjchem-1602	96	15	o2	o2	PROPN
eurjchem-1602	96	16	0.82	0.82	NUM
eurjchem-1602	96	17	2.34	2.34	NUM
eurjchem-1602	96	18	2.766(2	2.766(2	NUM
eurjchem-1602	96	19	)	)	PUNCT
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eurjchem-1602	96	21	c2	c2	PROPN
eurjchem-1602	96	22	h2b	h2b	PROPN
eurjchem-1602	96	23	o11	o11	VERB
eurjchem-1602	96	24	0.97	0.97	NUM
eurjchem-1602	96	25	2.55	2.55	NUM
eurjchem-1602	96	26	3.267(4	3.267(4	NUM
eurjchem-1602	96	27	)	)	PUNCT
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eurjchem-1602	96	29	1	1	NUM
eurjchem-1602	96	30	1‐x	1‐x	NOUN
eurjchem-1602	96	31	,	,	PUNCT
eurjchem-1602	96	32	‐1/2+y	‐1/2+y	X
eurjchem-1602	96	33	,	,	PUNCT
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eurjchem-1602	96	35	.	.	PUNCT
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eurjchem-1602	96	37	2	2	NUM
eurjchem-1602	96	38	.	.	PUNCT
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eurjchem-1602	96	44	1	1	NUM
eurjchem-1602	96	45	.	.	PUNCT
eurjchem-1602	97	1	in	in	ADP
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eurjchem-1602	97	3	,	,	PUNCT
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eurjchem-1602	97	8	these	these	DET
eurjchem-1602	97	9	two	two	NUM
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eurjchem-1602	97	12	will	will	AUX
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eurjchem-1602	97	15	.	.	PUNCT
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eurjchem-1602	98	2	the	the	DET
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eurjchem-1602	98	5	the	the	DET
eurjchem-1602	98	6	university	university	PROPN
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eurjchem-1602	98	9	(	(	PUNCT
eurjchem-1602	98	10	spain	spain	PROPN
eurjchem-1602	98	11	)	)	PUNCT
eurjchem-1602	98	12	and	and	CCONJ
eurjchem-1602	98	13	the	the	DET
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eurjchem-1602	98	15	fondation	fondation	PROPN
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eurjchem-1602	98	20	.	.	PUNCT
eurjchem-1602	99	1	supplementary	supplementary	ADJ
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eurjchem-1602	99	9	in	in	ADP
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eurjchem-1602	99	13	been	be	AUX
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eurjchem-1602	99	20	,	,	PUNCT
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eurjchem-1602	99	22	.	.	PUNCT
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eurjchem-1602	100	9	at	at	ADP
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eurjchem-1602	100	18	(	(	PUNCT
eurjchem-1602	100	19	ccdc	ccdc	PROPN
eurjchem-1602	100	20	)	)	PUNCT
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eurjchem-1602	101	1	12	12	NUM
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eurjchem-1602	101	14	336033	336033	NUM
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eurjchem-1602	101	17	:	:	PUNCT
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eurjchem-1602	103	2	,	,	PUNCT
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eurjchem-1602	103	4	,	,	PUNCT
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eurjchem-1602	103	6	.	.	PUNCT
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eurjchem-1602	104	4	.	.	PUNCT
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eurjchem-1602	108	33	;	;	PUNCT
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eurjchem-1602	108	42	.	.	PUNCT
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eurjchem-1602	111	4	.	.	PUNCT
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eurjchem-1602	111	8	;	;	PUNCT
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eurjchem-1602	113	2	.	.	PUNCT
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eurjchem-1602	117	2	,	,	PUNCT
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eurjchem-1602	124	3	,	,	PUNCT
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eurjchem-1602	128	6	.	.	PUNCT
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eurjchem-1602	129	4	.	.	PUNCT
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eurjchem-1602	130	2	,	,	PUNCT
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