id	sid	tid	token	lemma	pos
eurjchem-1635	1	1	untitled	untitle	VERB
eurjchem-1635	1	2	european	european	PROPN
eurjchem-1635	1	3	journal	journal	PROPN
eurjchem-1635	1	4	of	of	ADP
eurjchem-1635	1	5	chemistry	chemistry	NOUN
eurjchem-1635	1	6	8	8	NUM
eurjchem-1635	1	7	(	(	PUNCT
eurjchem-1635	1	8	4	4	NUM
eurjchem-1635	1	9	)	)	PUNCT
eurjchem-1635	1	10	(	(	PUNCT
eurjchem-1635	1	11	2017	2017	NUM
eurjchem-1635	1	12	)	)	PUNCT
eurjchem-1635	1	13	384‐390	384‐390	NUM
eurjchem-1635	1	14	european	european	ADJ
eurjchem-1635	1	15	journal	journal	PROPN
eurjchem-1635	1	16	of	of	ADP
eurjchem-1635	1	17	chemistry	chemistry	NOUN
eurjchem-1635	1	18	issn	issn	PROPN
eurjchem-1635	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-1635	1	20	(	(	PUNCT
eurjchem-1635	1	21	print	print	NOUN
eurjchem-1635	1	22	)	)	PUNCT
eurjchem-1635	1	23	/	/	SYM
eurjchem-1635	1	24	issn	issn	PROPN
eurjchem-1635	1	25	2153‐2257	2153‐2257	NUM
eurjchem-1635	1	26	(	(	PUNCT
eurjchem-1635	1	27	online	online	ADJ
eurjchem-1635	1	28	)	)	PUNCT
eurjchem-1635	1	29			NOUN
eurjchem-1635	1	30	2017	2017	NUM
eurjchem-1635	1	31	atlanta	atlanta	PROPN
eurjchem-1635	1	32	publishing	publishing	PROPN
eurjchem-1635	1	33	house	house	PROPN
eurjchem-1635	1	34	llc	llc	PROPN
eurjchem-1635	1	35	‐	‐	PUNCT
eurjchem-1635	1	36	all	all	DET
eurjchem-1635	1	37	rights	right	NOUN
eurjchem-1635	1	38	reserved	reserve	VERB
eurjchem-1635	1	39	‐	‐	NOUN
eurjchem-1635	1	40	printed	print	VERB
eurjchem-1635	1	41	in	in	ADP
eurjchem-1635	1	42	the	the	DET
eurjchem-1635	1	43	usa	usa	PROPN
eurjchem-1635	1	44	http://dx.doi.org/10.5155/eurjchem.8.4.384-390.1635	http://dx.doi.org/10.5155/eurjchem.8.4.384-390.1635	PROPN
eurjchem-1635	1	45	european	european	PROPN
eurjchem-1635	1	46	journal	journal	PROPN
eurjchem-1635	1	47	of	of	ADP
eurjchem-1635	1	48	chemistry	chemistry	PROPN
eurjchem-1635	1	49	journal	journal	PROPN
eurjchem-1635	1	50	webpage	webpage	NOUN
eurjchem-1635	1	51	:	:	PUNCT
eurjchem-1635	1	52	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1635	1	53	synthesis	synthesis	NOUN
eurjchem-1635	1	54	and	and	CCONJ
eurjchem-1635	1	55	antiproliferative	antiproliferative	ADJ
eurjchem-1635	1	56	evaluation	evaluation	NOUN
eurjchem-1635	1	57	of	of	ADP
eurjchem-1635	1	58	new	new	ADJ
eurjchem-1635	1	59	(	(	PUNCT
eurjchem-1635	1	60	4‐substituted‐3,4‐dihydro‐	4‐substituted‐3,4‐dihydro‐	NUM
eurjchem-1635	1	61	2h‐benzo[b][1,4]oxazin‐2‐yl)methane	2h‐benzo[b][1,4]oxazin‐2‐yl)methane	NOUN
eurjchem-1635	1	62	substituted	substitute	VERB
eurjchem-1635	1	63	sulfonamide	sulfonamide	NOUN
eurjchem-1635	1	64	derivatives	derivative	NOUN
eurjchem-1635	1	65	chandrakant	chandrakant	VERB
eurjchem-1635	1	66	dhondiram	dhondiram	PROPN
eurjchem-1635	1	67	pawar	pawar	PROPN
eurjchem-1635	1	68	1	1	NUM
eurjchem-1635	1	69	,	,	PUNCT
eurjchem-1635	1	70	*	*	PUNCT
eurjchem-1635	1	71	,	,	PUNCT
eurjchem-1635	1	72	aniket	aniket	PROPN
eurjchem-1635	1	73	sarkate	sarkate	VERB
eurjchem-1635	1	74	1	1	NUM
eurjchem-1635	1	75	,	,	PUNCT
eurjchem-1635	1	76	kshipra	kshipra	NOUN
eurjchem-1635	1	77	karnik	karnik	PROPN
eurjchem-1635	1	78	1	1	NUM
eurjchem-1635	1	79	,	,	PUNCT
eurjchem-1635	1	80	dattatraya	dattatraya	NOUN
eurjchem-1635	1	81	navnath	navnath	PROPN
eurjchem-1635	1	82	pansare	pansare	PROPN
eurjchem-1635	1	83	1	1	NUM
eurjchem-1635	1	84	and	and	CCONJ
eurjchem-1635	1	85	devanand	devanand	NOUN
eurjchem-1635	1	86	baburao	baburao	NOUN
eurjchem-1635	1	87	shinde	shinde	VERB
eurjchem-1635	1	88	2	2	NUM
eurjchem-1635	1	89	1	1	NUM
eurjchem-1635	1	90	department	department	NOUN
eurjchem-1635	1	91	of	of	ADP
eurjchem-1635	1	92	chemical	chemical	PROPN
eurjchem-1635	1	93	technology	technology	PROPN
eurjchem-1635	1	94	,	,	PUNCT
eurjchem-1635	1	95	dr	dr	PROPN
eurjchem-1635	1	96	.	.	PROPN
eurjchem-1635	1	97	babasaheb	babasaheb	PROPN
eurjchem-1635	1	98	ambedkar	ambedkar	PROPN
eurjchem-1635	1	99	marathwada	marathwada	PROPN
eurjchem-1635	1	100	university	university	PROPN
eurjchem-1635	1	101	,	,	PUNCT
eurjchem-1635	1	102	aurangabad	aurangabad	PROPN
eurjchem-1635	1	103	,	,	PUNCT
eurjchem-1635	1	104	431004	431004	NUM
eurjchem-1635	1	105	(	(	PUNCT
eurjchem-1635	1	106	ms	ms	NOUN
eurjchem-1635	1	107	)	)	PUNCT
eurjchem-1635	1	108	,	,	PUNCT
eurjchem-1635	1	109	india	india	PROPN
eurjchem-1635	1	110	2	2	NUM
eurjchem-1635	1	111	department	department	NOUN
eurjchem-1635	1	112	of	of	ADP
eurjchem-1635	1	113	chemistry	chemistry	NOUN
eurjchem-1635	1	114	,	,	PUNCT
eurjchem-1635	1	115	shivaji	shivaji	PROPN
eurjchem-1635	1	116	university	university	PROPN
eurjchem-1635	1	117	,	,	PUNCT
eurjchem-1635	1	118	vidyanagar	vidyanagar	NOUN
eurjchem-1635	1	119	,	,	PUNCT
eurjchem-1635	1	120	kolhapur	kolhapur	PROPN
eurjchem-1635	1	121	,	,	PUNCT
eurjchem-1635	1	122	416004	416004	NUM
eurjchem-1635	1	123	(	(	PUNCT
eurjchem-1635	1	124	ms	ms	NOUN
eurjchem-1635	1	125	)	)	PUNCT
eurjchem-1635	1	126	,	,	PUNCT
eurjchem-1635	1	127	india	india	PROPN
eurjchem-1635	1	128	*	*	PUNCT
eurjchem-1635	1	129	corresponding	correspond	VERB
eurjchem-1635	1	130	author	author	NOUN
eurjchem-1635	1	131	at	at	ADP
eurjchem-1635	1	132	:	:	PUNCT
eurjchem-1635	1	133	department	department	NOUN
eurjchem-1635	1	134	of	of	ADP
eurjchem-1635	1	135	chemical	chemical	PROPN
eurjchem-1635	1	136	technology	technology	PROPN
eurjchem-1635	1	137	,	,	PUNCT
eurjchem-1635	2	1	dr	dr	PROPN
eurjchem-1635	2	2	.	.	PROPN
eurjchem-1635	2	3	babasaheb	babasaheb	PROPN
eurjchem-1635	2	4	ambedkar	ambedkar	PROPN
eurjchem-1635	2	5	marathwada	marathwada	PROPN
eurjchem-1635	2	6	university	university	PROPN
eurjchem-1635	2	7	,	,	PUNCT
eurjchem-1635	2	8	aurangabad	aurangabad	PROPN
eurjchem-1635	2	9	,	,	PUNCT
eurjchem-1635	2	10	431004	431004	NUM
eurjchem-1635	2	11	(	(	PUNCT
eurjchem-1635	2	12	ms	ms	NOUN
eurjchem-1635	2	13	)	)	PUNCT
eurjchem-1635	2	14	,	,	PUNCT
eurjchem-1635	2	15	india	india	PROPN
eurjchem-1635	2	16	.	.	PUNCT
eurjchem-1635	3	1	tel	tel	PROPN
eurjchem-1635	3	2	.	.	PUNCT
eurjchem-1635	3	3	:	:	PUNCT
eurjchem-1635	4	1	+91.0240.2403308	+91.0240.2403308	X
eurjchem-1635	4	2	.	.	PUNCT
eurjchem-1635	5	1	fax	fax	NOUN
eurjchem-1635	5	2	:	:	PUNCT
eurjchem-1635	5	3	+91.0240.2400413	+91.0240.2400413	X
eurjchem-1635	5	4	.	.	PUNCT
eurjchem-1635	5	5	e‐mail	e‐mail	PUNCT
eurjchem-1635	6	1	address	address	NOUN
eurjchem-1635	6	2	:	:	PUNCT
eurjchem-1635	6	3	pawarcd2013@gmail.com	pawarcd2013@gmail.com	X
eurjchem-1635	6	4	(	(	PUNCT
eurjchem-1635	6	5	c.d	c.d	PROPN
eurjchem-1635	6	6	.	.	PROPN
eurjchem-1635	6	7	pawar	pawar	PROPN
eurjchem-1635	6	8	)	)	PUNCT
eurjchem-1635	6	9	.	.	PUNCT
eurjchem-1635	7	1	article	article	NOUN
eurjchem-1635	7	2	information	information	PROPN
eurjchem-1635	7	3	abstract	abstract	ADJ
eurjchem-1635	7	4	doi	doi	PROPN
eurjchem-1635	7	5	:	:	PUNCT
eurjchem-1635	7	6	 	 	SPACE
eurjchem-1635	7	7	10.5155	10.5155	NUM
eurjchem-1635	7	8	/	/	SYM
eurjchem-1635	7	9	eurjchem.8.4.384	eurjchem.8.4.384	PROPN
eurjchem-1635	7	10	-	-	NOUN
eurjchem-1635	7	11	390.1635	390.1635	NUM
eurjchem-1635	7	12	received	receive	VERB
eurjchem-1635	7	13	:	:	PUNCT
eurjchem-1635	7	14	01	01	NUM
eurjchem-1635	7	15	august	august	PROPN
eurjchem-1635	7	16	2017	2017	NUM
eurjchem-1635	7	17	received	receive	VERB
eurjchem-1635	7	18	in	in	ADP
eurjchem-1635	7	19	revised	revise	VERB
eurjchem-1635	7	20	form	form	NOUN
eurjchem-1635	7	21	:	:	PUNCT
eurjchem-1635	7	22	20	20	NUM
eurjchem-1635	7	23	september	september	PROPN
eurjchem-1635	7	24	2017	2017	NUM
eurjchem-1635	7	25	accepted	accept	VERB
eurjchem-1635	7	26	:	:	PUNCT
eurjchem-1635	7	27	23	23	NUM
eurjchem-1635	7	28	september	september	PROPN
eurjchem-1635	7	29	2017	2017	NUM
eurjchem-1635	7	30	published	publish	VERB
eurjchem-1635	7	31	online	online	ADV
eurjchem-1635	7	32	:	:	PUNCT
eurjchem-1635	7	33	31	31	NUM
eurjchem-1635	7	34	december	december	PROPN
eurjchem-1635	7	35	2017	2017	NUM
eurjchem-1635	7	36	printed	print	VERB
eurjchem-1635	7	37	:	:	PUNCT
eurjchem-1635	7	38	31	31	NUM
eurjchem-1635	7	39	december	december	PROPN
eurjchem-1635	7	40	2017	2017	NUM
eurjchem-1635	7	41	  	  	SPACE
eurjchem-1635	7	42	a	a	DET
eurjchem-1635	7	43	series	series	NOUN
eurjchem-1635	7	44	of	of	ADP
eurjchem-1635	7	45	new	new	ADJ
eurjchem-1635	7	46	molecules	molecule	NOUN
eurjchem-1635	7	47	having	have	VERB
eurjchem-1635	7	48	4‐substituted‐3,4‐dihydro‐2h‐benzo[b][1,4]oxazin‐2‐	4‐substituted‐3,4‐dihydro‐2h‐benzo[b][1,4]oxazin‐2‐	NUM
eurjchem-1635	7	49	yl)methane	yl)methane	NOUN
eurjchem-1635	7	50	substituted	substitute	VERB
eurjchem-1635	7	51	sulfonamide	sulfonamide	NOUN
eurjchem-1635	7	52	derivatives	derivative	NOUN
eurjchem-1635	7	53	were	be	AUX
eurjchem-1635	7	54	synthesized	synthesize	VERB
eurjchem-1635	7	55	.	.	PUNCT
eurjchem-1635	8	1	the	the	DET
eurjchem-1635	8	2	structures	structure	NOUN
eurjchem-1635	8	3	of	of	ADP
eurjchem-1635	8	4	the	the	DET
eurjchem-1635	8	5	synthesized	synthesize	VERB
eurjchem-1635	8	6	compounds	compound	NOUN
eurjchem-1635	8	7	were	be	AUX
eurjchem-1635	8	8	elucidated	elucidate	VERB
eurjchem-1635	8	9	and	and	CCONJ
eurjchem-1635	8	10	confirmed	confirm	VERB
eurjchem-1635	8	11	by	by	ADP
eurjchem-1635	8	12	1h	1h	NUM
eurjchem-1635	8	13	nmr	nmr	NOUN
eurjchem-1635	8	14	,	,	PUNCT
eurjchem-1635	8	15	13c	13c	NOUN
eurjchem-1635	8	16	nmr	nmr	NOUN
eurjchem-1635	8	17	,	,	PUNCT
eurjchem-1635	8	18	mass	mass	NOUN
eurjchem-1635	8	19	spectra	spectra	NOUN
eurjchem-1635	8	20	,	,	PUNCT
eurjchem-1635	8	21	and	and	CCONJ
eurjchem-1635	8	22	the	the	DET
eurjchem-1635	8	23	purity	purity	NOUN
eurjchem-1635	8	24	was	be	AUX
eurjchem-1635	8	25	checked	check	VERB
eurjchem-1635	8	26	through	through	ADP
eurjchem-1635	8	27	hplc	hplc	NOUN
eurjchem-1635	8	28	analysis	analysis	NOUN
eurjchem-1635	8	29	.	.	PUNCT
eurjchem-1635	9	1	the	the	DET
eurjchem-1635	9	2	compounds	compound	NOUN
eurjchem-1635	9	3	were	be	AUX
eurjchem-1635	9	4	also	also	ADV
eurjchem-1635	9	5	evaluated	evaluate	VERB
eurjchem-1635	9	6	for	for	ADP
eurjchem-1635	9	7	their	their	PRON
eurjchem-1635	9	8	in	in	X
eurjchem-1635	9	9	vitro	vitro	X
eurjchem-1635	9	10	antiproliferative	antiproliferative	ADJ
eurjchem-1635	9	11	activity	activity	NOUN
eurjchem-1635	9	12	against	against	ADP
eurjchem-1635	9	13	mcf‐7	mcf‐7	PROPN
eurjchem-1635	9	14	,	,	PUNCT
eurjchem-1635	9	15	hela	hela	PROPN
eurjchem-1635	9	16	,	,	PUNCT
eurjchem-1635	9	17	a‐549	a‐549	NOUN
eurjchem-1635	9	18	and	and	CCONJ
eurjchem-1635	9	19	du‐145	du‐145	NOUN
eurjchem-1635	9	20	cancer	cancer	NOUN
eurjchem-1635	9	21	cell	cell	NOUN
eurjchem-1635	9	22	lines	line	NOUN
eurjchem-1635	9	23	by	by	ADP
eurjchem-1635	9	24	mtt	mtt	NOUN
eurjchem-1635	9	25	assay	assay	NOUN
eurjchem-1635	9	26	.	.	PUNCT
eurjchem-1635	10	1	compounds	compound	VERB
eurjchem-1635	10	2	4d	4d	NUM
eurjchem-1635	10	3	,	,	PUNCT
eurjchem-1635	10	4	7c	7c	PROPN
eurjchem-1635	10	5	and	and	CCONJ
eurjchem-1635	10	6	7d	7d	NUM
eurjchem-1635	10	7	were	be	AUX
eurjchem-1635	10	8	tested	test	VERB
eurjchem-1635	10	9	for	for	ADP
eurjchem-1635	10	10	their	their	PRON
eurjchem-1635	10	11	activity	activity	NOUN
eurjchem-1635	10	12	against	against	ADP
eurjchem-1635	10	13	a	a	DET
eurjchem-1635	10	14	panel	panel	NOUN
eurjchem-1635	10	15	of	of	ADP
eurjchem-1635	10	16	eight	eight	NUM
eurjchem-1635	10	17	human	human	ADJ
eurjchem-1635	10	18	kinase	kinase	NOUN
eurjchem-1635	10	19	at	at	ADP
eurjchem-1635	10	20	10	10	NUM
eurjchem-1635	10	21	µm	µm	ADP
eurjchem-1635	10	22	concentrations	concentration	NOUN
eurjchem-1635	10	23	.	.	PUNCT
eurjchem-1635	11	1	among	among	ADP
eurjchem-1635	11	2	them	they	PRON
eurjchem-1635	11	3	the	the	DET
eurjchem-1635	11	4	compounds	compound	NOUN
eurjchem-1635	11	5	4d	4d	NOUN
eurjchem-1635	11	6	and	and	CCONJ
eurjchem-1635	11	7	7d	7d	NOUN
eurjchem-1635	11	8	showed	show	VERB
eurjchem-1635	11	9	very	very	ADV
eurjchem-1635	11	10	promising	promising	ADJ
eurjchem-1635	11	11	activity	activity	NOUN
eurjchem-1635	11	12	against	against	ADP
eurjchem-1635	11	13	cdk5	cdk5	PROPN
eurjchem-1635	11	14	/	/	SYM
eurjchem-1635	11	15	p25	p25	PROPN
eurjchem-1635	11	16	kinase	kinase	NOUN
eurjchem-1635	11	17	with	with	ADP
eurjchem-1635	11	18	66	66	NUM
eurjchem-1635	11	19	and	and	CCONJ
eurjchem-1635	11	20	70	70	NUM
eurjchem-1635	11	21	%	%	NOUN
eurjchem-1635	11	22	inhibitions	inhibition	NOUN
eurjchem-1635	11	23	,	,	PUNCT
eurjchem-1635	11	24	respectively	respectively	ADV
eurjchem-1635	11	25	.	.	PUNCT
eurjchem-1635	12	1	compound	compound	NOUN
eurjchem-1635	12	2	7c	7c	PROPN
eurjchem-1635	12	3	also	also	ADV
eurjchem-1635	12	4	showed	show	VERB
eurjchem-1635	12	5	promising	promising	ADJ
eurjchem-1635	12	6	activity	activity	NOUN
eurjchem-1635	12	7	of	of	ADP
eurjchem-1635	12	8	59	59	NUM
eurjchem-1635	12	9	%	%	NOUN
eurjchem-1635	12	10	inhibition	inhibition	NOUN
eurjchem-1635	12	11	.	.	PUNCT
eurjchem-1635	13	1	the	the	DET
eurjchem-1635	13	2	preliminary	preliminary	ADJ
eurjchem-1635	13	3	bioassay	bioassay	NOUN
eurjchem-1635	13	4	showed	show	VERB
eurjchem-1635	13	5	that	that	SCONJ
eurjchem-1635	13	6	most	most	ADJ
eurjchem-1635	13	7	of	of	ADP
eurjchem-1635	13	8	the	the	DET
eurjchem-1635	13	9	compounds	compound	NOUN
eurjchem-1635	13	10	were	be	AUX
eurjchem-1635	13	11	antiproliferative	antiproliferative	ADJ
eurjchem-1635	13	12	with	with	ADP
eurjchem-1635	13	13	different	different	ADJ
eurjchem-1635	13	14	degrees	degree	NOUN
eurjchem-1635	13	15	,	,	PUNCT
eurjchem-1635	13	16	and	and	CCONJ
eurjchem-1635	13	17	some	some	DET
eurjchem-1635	13	18	compounds	compound	NOUN
eurjchem-1635	13	19	showed	show	VERB
eurjchem-1635	13	20	better	well	ADJ
eurjchem-1635	13	21	activity	activity	NOUN
eurjchem-1635	13	22	than	than	ADP
eurjchem-1635	13	23	5‐fluorouracil	5‐fluorouracil	NUM
eurjchem-1635	13	24	which	which	PRON
eurjchem-1635	13	25	was	be	AUX
eurjchem-1635	13	26	used	use	VERB
eurjchem-1635	13	27	as	as	ADP
eurjchem-1635	13	28	positive	positive	ADJ
eurjchem-1635	13	29	control	control	NOUN
eurjchem-1635	13	30	.	.	PUNCT
eurjchem-1635	14	1	keywords	keyword	NOUN
eurjchem-1635	14	2	benzoxazine	benzoxazine	VERB
eurjchem-1635	14	3	human	human	PROPN
eurjchem-1635	14	4	kinase	kinase	PROPN
eurjchem-1635	14	5	antiproliferative	antiproliferative	NOUN
eurjchem-1635	14	6	sulfonyl	sulfonyl	PROPN
eurjchem-1635	14	7	chlorides	chloride	NOUN
eurjchem-1635	14	8	phenylmethanethiol	phenylmethanethiol	PROPN
eurjchem-1635	14	9	cdk5	cdk5	PROPN
eurjchem-1635	14	10	/	/	SYM
eurjchem-1635	14	11	p25	p25	PROPN
eurjchem-1635	14	12	kinase	kinase	NOUN
eurjchem-1635	14	13	inhibitors	inhibitor	NOUN
eurjchem-1635	14	14	cite	cite	VERB
eurjchem-1635	14	15	this	this	PRON
eurjchem-1635	14	16	:	:	PUNCT
eurjchem-1635	14	17	eur	eur	PROPN
eurjchem-1635	14	18	.	.	PUNCT
eurjchem-1635	15	1	j.	j.	PROPN
eurjchem-1635	15	2	chem	chem	PROPN
eurjchem-1635	15	3	.	.	PUNCT
eurjchem-1635	16	1	2017	2017	NUM
eurjchem-1635	16	2	,	,	PUNCT
eurjchem-1635	16	3	8(4	8(4	NUM
eurjchem-1635	16	4	)	)	PUNCT
eurjchem-1635	16	5	,	,	PUNCT
eurjchem-1635	16	6	384‐390	384‐390	NUM
eurjchem-1635	16	7	1	1	NUM
eurjchem-1635	16	8	.	.	PUNCT
eurjchem-1635	16	9	introduction	introduction	NOUN
eurjchem-1635	16	10	cancer	cancer	NOUN
eurjchem-1635	16	11	is	be	AUX
eurjchem-1635	16	12	the	the	DET
eurjchem-1635	16	13	major	major	ADJ
eurjchem-1635	16	14	threat	threat	NOUN
eurjchem-1635	16	15	globally	globally	ADV
eurjchem-1635	16	16	in	in	ADP
eurjchem-1635	16	17	20th	20th	ADJ
eurjchem-1635	16	18	century	century	NOUN
eurjchem-1635	16	19	.	.	PUNCT
eurjchem-1635	17	1	its	its	PRON
eurjchem-1635	17	2	treatment	treatment	NOUN
eurjchem-1635	17	3	is	be	AUX
eurjchem-1635	17	4	difficult	difficult	ADJ
eurjchem-1635	17	5	due	due	ADJ
eurjchem-1635	17	6	to	to	ADP
eurjchem-1635	17	7	concerns	concern	NOUN
eurjchem-1635	17	8	about	about	ADP
eurjchem-1635	17	9	the	the	DET
eurjchem-1635	17	10	toxicity	toxicity	NOUN
eurjchem-1635	17	11	and	and	CCONJ
eurjchem-1635	17	12	side	side	NOUN
eurjchem-1635	17	13	effects	effect	NOUN
eurjchem-1635	17	14	[	[	X
eurjchem-1635	17	15	1	1	NUM
eurjchem-1635	17	16	]	]	PUNCT
eurjchem-1635	17	17	.	.	PUNCT
eurjchem-1635	18	1	therefore	therefore	ADV
eurjchem-1635	18	2	,	,	PUNCT
eurjchem-1635	18	3	a	a	DET
eurjchem-1635	18	4	good	good	ADJ
eurjchem-1635	18	5	deal	deal	NOUN
eurjchem-1635	18	6	of	of	ADP
eurjchem-1635	18	7	interest	interest	NOUN
eurjchem-1635	18	8	has	have	AUX
eurjchem-1635	18	9	develop‐	develop‐	NOUN
eurjchem-1635	18	10	ped	pe	VERB
eurjchem-1635	18	11	among	among	ADP
eurjchem-1635	18	12	the	the	DET
eurjchem-1635	18	13	medicinal	medicinal	ADJ
eurjchem-1635	18	14	chemists	chemist	NOUN
eurjchem-1635	18	15	for	for	ADP
eurjchem-1635	18	16	the	the	DET
eurjchem-1635	18	17	design	design	NOUN
eurjchem-1635	18	18	,	,	PUNCT
eurjchem-1635	18	19	discovery	discovery	NOUN
eurjchem-1635	18	20	and	and	CCONJ
eurjchem-1635	18	21	development	development	NOUN
eurjchem-1635	18	22	of	of	ADP
eurjchem-1635	18	23	more	more	ADV
eurjchem-1635	18	24	selective	selective	ADJ
eurjchem-1635	18	25	anticancer	anticancer	NOUN
eurjchem-1635	18	26	agents	agent	NOUN
eurjchem-1635	18	27	having	have	VERB
eurjchem-1635	18	28	fewer	few	ADJ
eurjchem-1635	18	29	side	side	ADJ
eurjchem-1635	18	30	effects	effect	NOUN
eurjchem-1635	18	31	[	[	X
eurjchem-1635	18	32	2,3	2,3	NUM
eurjchem-1635	18	33	]	]	PUNCT
eurjchem-1635	18	34	.	.	PUNCT
eurjchem-1635	19	1	various	various	ADJ
eurjchem-1635	19	2	types	type	NOUN
eurjchem-1635	19	3	of	of	ADP
eurjchem-1635	19	4	anticancer	anticancer	NOUN
eurjchem-1635	19	5	drugs	drug	NOUN
eurjchem-1635	19	6	have	have	VERB
eurjchem-1635	19	7	diverse	diverse	ADJ
eurjchem-1635	19	8	mechanism	mechanism	NOUN
eurjchem-1635	19	9	of	of	ADP
eurjchem-1635	19	10	action	action	NOUN
eurjchem-1635	19	11	on	on	ADP
eurjchem-1635	19	12	the	the	DET
eurjchem-1635	19	13	cancerous	cancerous	ADJ
eurjchem-1635	19	14	cells	cell	NOUN
eurjchem-1635	19	15	.	.	PUNCT
eurjchem-1635	20	1	hence	hence	ADV
eurjchem-1635	20	2	,	,	PUNCT
eurjchem-1635	20	3	finding	find	VERB
eurjchem-1635	20	4	out	out	ADP
eurjchem-1635	20	5	such	such	ADJ
eurjchem-1635	20	6	mechanisms	mechanism	NOUN
eurjchem-1635	20	7	will	will	AUX
eurjchem-1635	20	8	be	be	AUX
eurjchem-1635	20	9	helpful	helpful	ADJ
eurjchem-1635	20	10	in	in	ADP
eurjchem-1635	20	11	the	the	DET
eurjchem-1635	20	12	designing	designing	NOUN
eurjchem-1635	20	13	of	of	ADP
eurjchem-1635	20	14	suitable	suitable	ADJ
eurjchem-1635	20	15	curative	curative	ADJ
eurjchem-1635	20	16	remedy	remedy	NOUN
eurjchem-1635	20	17	for	for	ADP
eurjchem-1635	20	18	attacking	attack	VERB
eurjchem-1635	20	19	the	the	DET
eurjchem-1635	20	20	cancerous	cancerous	ADJ
eurjchem-1635	20	21	cells	cell	NOUN
eurjchem-1635	20	22	[	[	X
eurjchem-1635	20	23	4	4	NUM
eurjchem-1635	20	24	]	]	PUNCT
eurjchem-1635	20	25	.	.	PUNCT
eurjchem-1635	21	1	here	here	ADV
eurjchem-1635	21	2	we	we	PRON
eurjchem-1635	21	3	have	have	AUX
eurjchem-1635	21	4	chosen	choose	VERB
eurjchem-1635	21	5	benzo[b][1,4]oxazinyl	benzo[b][1,4]oxazinyl	NOUN
eurjchem-1635	21	6	class	class	NOUN
eurjchem-1635	21	7	for	for	ADP
eurjchem-1635	21	8	the	the	DET
eurjchem-1635	21	9	synthesis	synthesis	NOUN
eurjchem-1635	21	10	as	as	SCONJ
eurjchem-1635	21	11	these	these	DET
eurjchem-1635	21	12	derivatives	derivative	NOUN
eurjchem-1635	21	13	have	have	VERB
eurjchem-1635	21	14	a	a	DET
eurjchem-1635	21	15	wide	wide	ADJ
eurjchem-1635	21	16	range	range	NOUN
eurjchem-1635	21	17	of	of	ADP
eurjchem-1635	21	18	biological	biological	ADJ
eurjchem-1635	21	19	activities	activity	NOUN
eurjchem-1635	21	20	like	like	VERB
eurjchem-1635	21	21	,	,	PUNCT
eurjchem-1635	21	22	treatment	treatment	NOUN
eurjchem-1635	21	23	of	of	ADP
eurjchem-1635	21	24	cardiovascular	cardiovascular	ADJ
eurjchem-1635	22	1	[	[	X
eurjchem-1635	22	2	5‐7	5‐7	PROPN
eurjchem-1635	22	3	]	]	X
eurjchem-1635	22	4	,	,	PUNCT
eurjchem-1635	22	5	antibacterial	antibacterial	ADJ
eurjchem-1635	22	6	[	[	X
eurjchem-1635	22	7	8,9	8,9	NUM
eurjchem-1635	22	8	]	]	PUNCT
eurjchem-1635	22	9	,	,	PUNCT
eurjchem-1635	22	10	antifungal	antifungal	PROPN
eurjchem-1635	23	1	[	[	X
eurjchem-1635	23	2	10‐12	10‐12	NUM
eurjchem-1635	23	3	]	]	PUNCT
eurjchem-1635	23	4	,	,	PUNCT
eurjchem-1635	23	5	anticancer	anticancer	NOUN
eurjchem-1635	23	6	activity	activity	NOUN
eurjchem-1635	24	1	[	[	X
eurjchem-1635	24	2	13‐15	13‐15	NUM
eurjchem-1635	24	3	]	]	PUNCT
eurjchem-1635	24	4	and	and	CCONJ
eurjchem-1635	24	5	pro‐	pro‐	PROPN
eurjchem-1635	24	6	tein	tein	NOUN
eurjchem-1635	24	7	methyl	methyl	NOUN
eurjchem-1635	24	8	transferases	transferase	NOUN
eurjchem-1635	24	9	inhibitors	inhibitor	NOUN
eurjchem-1635	24	10	[	[	X
eurjchem-1635	24	11	16	16	NUM
eurjchem-1635	24	12	]	]	PUNCT
eurjchem-1635	24	13	.	.	PUNCT
eurjchem-1635	25	1	sulphonamide	sulphonamide	PROPN
eurjchem-1635	25	2	deriva‐	deriva‐	PROPN
eurjchem-1635	25	3	tives	tive	NOUN
eurjchem-1635	25	4	are	be	AUX
eurjchem-1635	25	5	considered	consider	VERB
eurjchem-1635	25	6	as	as	ADP
eurjchem-1635	25	7	an	an	DET
eurjchem-1635	25	8	important	important	ADJ
eurjchem-1635	25	9	moiety	moiety	NOUN
eurjchem-1635	25	10	in	in	ADP
eurjchem-1635	25	11	drug	drug	NOUN
eurjchem-1635	25	12	synthesis	synthesis	NOUN
eurjchem-1635	25	13	and	and	CCONJ
eurjchem-1635	25	14	have	have	VERB
eurjchem-1635	25	15	excellent	excellent	ADJ
eurjchem-1635	25	16	antimicrobial	antimicrobial	ADJ
eurjchem-1635	25	17	activity	activity	NOUN
eurjchem-1635	26	1	[	[	X
eurjchem-1635	26	2	17	17	NUM
eurjchem-1635	26	3	]	]	PUNCT
eurjchem-1635	26	4	.	.	PUNCT
eurjchem-1635	27	1	literature	literature	NOUN
eurjchem-1635	27	2	survey	survey	NOUN
eurjchem-1635	27	3	reveals	reveal	VERB
eurjchem-1635	27	4	that	that	SCONJ
eurjchem-1635	27	5	sulphonamide	sulphonamide	NOUN
eurjchem-1635	27	6	bearing	bear	VERB
eurjchem-1635	27	7	drug	drug	NOUN
eurjchem-1635	27	8	molecules	molecule	NOUN
eurjchem-1635	27	9	like	like	ADP
eurjchem-1635	27	10	dihydropyrazole	dihydropyrazole	NOUN
eurjchem-1635	27	11	sulphonamide	sulphonamide	NOUN
eurjchem-1635	27	12	derivatives	derivative	NOUN
eurjchem-1635	27	13	[	[	X
eurjchem-1635	27	14	18	18	NUM
eurjchem-1635	27	15	]	]	PUNCT
eurjchem-1635	27	16	and	and	CCONJ
eurjchem-1635	27	17	pyrazoline	pyrazoline	NOUN
eurjchem-1635	27	18	substituted	substitute	VERB
eurjchem-1635	27	19	benzenesulfonylureas	benzenesulfonylurea	NOUN
eurjchem-1635	28	1	[	[	X
eurjchem-1635	28	2	19	19	NUM
eurjchem-1635	28	3	]	]	PUNCT
eurjchem-1635	28	4	act	act	NOUN
eurjchem-1635	28	5	as	as	ADP
eurjchem-1635	28	6	potential	potential	ADJ
eurjchem-1635	28	7	cox‐1	cox‐1	PROPN
eurjchem-1635	28	8	/	/	SYM
eurjchem-1635	28	9	cox‐2	cox‐2	NOUN
eurjchem-1635	28	10	inhibitors	inhibitor	NOUN
eurjchem-1635	28	11	and	and	CCONJ
eurjchem-1635	28	12	antiproloferative	antiproloferative	ADJ
eurjchem-1635	28	13	agents	agent	NOUN
eurjchem-1635	28	14	,	,	PUNCT
eurjchem-1635	28	15	respectively	respectively	ADV
eurjchem-1635	28	16	.	.	PUNCT
eurjchem-1635	29	1	our	our	PRON
eurjchem-1635	29	2	research	research	NOUN
eurjchem-1635	29	3	group	group	NOUN
eurjchem-1635	29	4	previously	previously	ADV
eurjchem-1635	29	5	reported	report	VERB
eurjchem-1635	29	6	antimicrobial	antimicrobial	ADJ
eurjchem-1635	29	7	and	and	CCONJ
eurjchem-1635	29	8	anticancer	anticancer	NOUN
eurjchem-1635	29	9	evaluation	evaluation	NOUN
eurjchem-1635	29	10	for	for	ADP
eurjchem-1635	29	11	new	new	ADJ
eurjchem-1635	29	12	derivatives	derivative	NOUN
eurjchem-1635	29	13	of	of	ADP
eurjchem-1635	29	14	thiazole	thiazole	NOUN
eurjchem-1635	29	15	,	,	PUNCT
eurjchem-1635	29	16	piperidone	piperidone	NOUN
eurjchem-1635	29	17	and	and	CCONJ
eurjchem-1635	29	18	thiazolidinone	thiazolidinone	NOUN
eurjchem-1635	29	19	[	[	X
eurjchem-1635	29	20	20,21	20,21	NUM
eurjchem-1635	29	21	]	]	PUNCT
eurjchem-1635	29	22	.	.	PUNCT
eurjchem-1635	30	1	recent	recent	ADJ
eurjchem-1635	30	2	literature	literature	NOUN
eurjchem-1635	30	3	reveals	reveal	VERB
eurjchem-1635	30	4	the	the	DET
eurjchem-1635	30	5	synthesis	synthesis	NOUN
eurjchem-1635	30	6	of	of	ADP
eurjchem-1635	30	7	1,4‐oxazine‐2‐yl	1,4‐oxazine‐2‐yl	NUM
eurjchem-1635	30	8	derivatives	derivative	NOUN
eurjchem-1635	30	9	in	in	ADP
eurjchem-1635	30	10	water	water	NOUN
eurjchem-1635	30	11	as	as	ADP
eurjchem-1635	30	12	green	green	ADJ
eurjchem-1635	30	13	solvent	solvent	NOUN
eurjchem-1635	31	1	[	[	X
eurjchem-1635	31	2	22	22	NUM
eurjchem-1635	31	3	]	]	PUNCT
eurjchem-1635	31	4	.	.	PUNCT
eurjchem-1635	32	1	in	in	ADP
eurjchem-1635	32	2	continuation	continuation	NOUN
eurjchem-1635	32	3	of	of	ADP
eurjchem-1635	32	4	our	our	PRON
eurjchem-1635	32	5	research	research	NOUN
eurjchem-1635	32	6	and	and	CCONJ
eurjchem-1635	32	7	owing	owe	VERB
eurjchem-1635	32	8	to	to	ADP
eurjchem-1635	32	9	the	the	DET
eurjchem-1635	32	10	advantages	advantage	NOUN
eurjchem-1635	32	11	of	of	ADP
eurjchem-1635	32	12	benzo[b][1,4	benzo[b][1,4	NOUN
eurjchem-1635	32	13	]	]	X
eurjchem-1635	32	14	oxazinyl	oxazinyl	NOUN
eurjchem-1635	32	15	as	as	ADV
eurjchem-1635	32	16	well	well	ADV
eurjchem-1635	32	17	as	as	ADP
eurjchem-1635	32	18	sulphonamide	sulphonamide	NOUN
eurjchem-1635	32	19	moieties	moiety	NOUN
eurjchem-1635	32	20	,	,	PUNCT
eurjchem-1635	32	21	we	we	PRON
eurjchem-1635	32	22	have	have	AUX
eurjchem-1635	32	23	synthe‐	synthe‐	AUX
eurjchem-1635	32	24	sized	size	VERB
eurjchem-1635	32	25	new	new	ADJ
eurjchem-1635	32	26	derivatives	derivative	NOUN
eurjchem-1635	32	27	containing	contain	VERB
eurjchem-1635	32	28	sulfonamide	sulfonamide	NOUN
eurjchem-1635	32	29	and	and	CCONJ
eurjchem-1635	32	30	benzo[b	benzo[b	NOUN
eurjchem-1635	32	31	]	]	PUNCT
eurjchem-1635	33	1	[	[	X
eurjchem-1635	33	2	1,4]oxazinyl	1,4]oxazinyl	NOUN
eurjchem-1635	33	3	in	in	ADP
eurjchem-1635	33	4	one	one	NUM
eurjchem-1635	33	5	frame	frame	NOUN
eurjchem-1635	33	6	work	work	NOUN
eurjchem-1635	33	7	.	.	PUNCT
eurjchem-1635	34	1	the	the	DET
eurjchem-1635	34	2	synthetic	synthetic	ADJ
eurjchem-1635	34	3	methods	method	NOUN
eurjchem-1635	34	4	adop‐	adop‐	NOUN
eurjchem-1635	34	5	ted	te	VERB
eurjchem-1635	34	6	for	for	ADP
eurjchem-1635	34	7	the	the	DET
eurjchem-1635	34	8	preparation	preparation	NOUN
eurjchem-1635	34	9	of	of	ADP
eurjchem-1635	34	10	the	the	DET
eurjchem-1635	34	11	4‐substituted‐3,4‐dihydro‐2h‐	4‐substituted‐3,4‐dihydro‐2h‐	PROPN
eurjchem-1635	34	12	benzo[b][1,4	benzo[b][1,4	PROPN
eurjchem-1635	34	13	]	]	PUNCT
eurjchem-1635	35	1	oxazin‐2‐yl)methane	oxazin‐2‐yl)methane	NOUN
eurjchem-1635	35	2	substituted	substitute	VERB
eurjchem-1635	35	3	sulfonamide	sulfonamide	NOUN
eurjchem-1635	35	4	derivatives	derivative	NOUN
eurjchem-1635	35	5	(	(	PUNCT
eurjchem-1635	35	6	4a‐e	4a‐e	NOUN
eurjchem-1635	35	7	and	and	CCONJ
eurjchem-1635	35	8	7a‐e	7a‐e	PROPN
eurjchem-1635	35	9	)	)	PUNCT
eurjchem-1635	35	10	are	be	AUX
eurjchem-1635	35	11	depicted	depict	VERB
eurjchem-1635	35	12	in	in	ADP
eurjchem-1635	35	13	scheme	scheme	NOUN
eurjchem-1635	35	14	1	1	NUM
eurjchem-1635	35	15	and	and	CCONJ
eurjchem-1635	35	16	2	2	NUM
eurjchem-1635	35	17	presented	present	VERB
eurjchem-1635	35	18	below	below	ADV
eurjchem-1635	35	19	.	.	PUNCT
eurjchem-1635	36	1	these	these	DET
eurjchem-1635	36	2	derivatives	derivative	NOUN
eurjchem-1635	36	3	are	be	AUX
eurjchem-1635	36	4	screened	screen	VERB
eurjchem-1635	36	5	against	against	ADP
eurjchem-1635	36	6	a	a	DET
eurjchem-1635	36	7	series	series	NOUN
eurjchem-1635	36	8	of	of	ADP
eurjchem-1635	36	9	five	five	NUM
eurjchem-1635	36	10	anticancer	anticancer	NOUN
eurjchem-1635	36	11	cell	cell	NOUN
eurjchem-1635	36	12	lines	line	NOUN
eurjchem-1635	36	13	and	and	CCONJ
eurjchem-1635	36	14	some	some	PRON
eurjchem-1635	36	15	were	be	AUX
eurjchem-1635	36	16	tested	test	VERB
eurjchem-1635	36	17	for	for	ADP
eurjchem-1635	36	18	its	its	PRON
eurjchem-1635	36	19	activity	activity	NOUN
eurjchem-1635	36	20	against	against	ADP
eurjchem-1635	36	21	a	a	DET
eurjchem-1635	36	22	panel	panel	NOUN
eurjchem-1635	36	23	of	of	ADP
eurjchem-1635	36	24	eight	eight	NUM
eurjchem-1635	36	25	human	human	ADJ
eurjchem-1635	36	26	kinase	kinase	NOUN
eurjchem-1635	36	27	at	at	ADP
eurjchem-1635	36	28	10	10	NUM
eurjchem-1635	36	29	µm	µm	ADP
eurjchem-1635	36	30	concentrations	concentration	NOUN
eurjchem-1635	36	31	.	.	PUNCT
eurjchem-1635	37	1	by	by	ADP
eurjchem-1635	37	2	considering	consider	VERB
eurjchem-1635	37	3	the	the	DET
eurjchem-1635	37	4	biological	biological	ADJ
eurjchem-1635	37	5	importance	importance	NOUN
eurjchem-1635	37	6	of	of	ADP
eurjchem-1635	37	7	sulfonamides	sulfonamide	NOUN
eurjchem-1635	37	8	,	,	PUNCT
eurjchem-1635	37	9	we	we	PRON
eurjchem-1635	37	10	have	have	AUX
eurjchem-1635	37	11	synthesized	synthesize	VERB
eurjchem-1635	37	12	series	series	NOUN
eurjchem-1635	37	13	of	of	ADP
eurjchem-1635	37	14	compounds	compound	NOUN
eurjchem-1635	37	15	having	have	VERB
eurjchem-1635	37	16	4‐substituted‐3,4‐dihydro‐2h‐benzo[b][1,4]oxazin‐2‐	4‐substituted‐3,4‐dihydro‐2h‐benzo[b][1,4]oxazin‐2‐	NUM
eurjchem-1635	37	17	yl)methane	yl)methane	NOUN
eurjchem-1635	37	18	substituted	substitute	VERB
eurjchem-1635	37	19	sulfonamide	sulfonamide	NOUN
eurjchem-1635	37	20	derivatives	derivative	NOUN
eurjchem-1635	37	21	,	,	PUNCT
eurjchem-1635	37	22	4a‐e	4a‐e	NOUN
eurjchem-1635	37	23	and	and	CCONJ
eurjchem-1635	37	24	7a‐	7a‐	NUM
eurjchem-1635	37	25	e.	e.	PROPN
eurjchem-1635	37	26	2	2	PROPN
eurjchem-1635	37	27	.	.	PUNCT
eurjchem-1635	37	28	experimental	experimental	ADJ
eurjchem-1635	37	29	2.1	2.1	NUM
eurjchem-1635	37	30	.	.	PUNCT
eurjchem-1635	38	1	chemicals	chemical	NOUN
eurjchem-1635	38	2	and	and	CCONJ
eurjchem-1635	38	3	instrumentation	instrumentation	NOUN
eurjchem-1635	38	4	pawar	pawar	PROPN
eurjchem-1635	38	5	et	et	PROPN
eurjchem-1635	38	6	al	al	PROPN
eurjchem-1635	38	7	.	.	PUNCT
eurjchem-1635	38	8	/	/	SYM
eurjchem-1635	38	9	european	european	PROPN
eurjchem-1635	38	10	journal	journal	PROPN
eurjchem-1635	38	11	of	of	ADP
eurjchem-1635	38	12	chemistry	chemistry	NOUN
eurjchem-1635	38	13	8	8	NUM
eurjchem-1635	38	14	(	(	PUNCT
eurjchem-1635	38	15	4	4	NUM
eurjchem-1635	38	16	)	)	PUNCT
eurjchem-1635	38	17	(	(	PUNCT
eurjchem-1635	38	18	2017	2017	NUM
eurjchem-1635	38	19	)	)	PUNCT
eurjchem-1635	38	20	384‐390	384‐390	NUM
eurjchem-1635	38	21	385	385	NUM
eurjchem-1635	38	22	reagents	reagent	NOUN
eurjchem-1635	38	23	and	and	CCONJ
eurjchem-1635	38	24	conditions	condition	NOUN
eurjchem-1635	38	25	:	:	PUNCT
eurjchem-1635	38	26	(	(	PUNCT
eurjchem-1635	38	27	a	a	X
eurjchem-1635	38	28	)	)	PUNCT
eurjchem-1635	38	29	2‐chloroacrylonitrile	2‐chloroacrylonitrile	ADJ
eurjchem-1635	38	30	,	,	PUNCT
eurjchem-1635	38	31	cs2co3	cs2co3	ADJ
eurjchem-1635	38	32	,	,	PUNCT
eurjchem-1635	38	33	toluene	toluene	NOUN
eurjchem-1635	38	34	,	,	PUNCT
eurjchem-1635	38	35	60	60	NUM
eurjchem-1635	38	36	°	°	NOUN
eurjchem-1635	38	37	c	c	NOUN
eurjchem-1635	38	38	,	,	PUNCT
eurjchem-1635	38	39	0.5	0.5	NUM
eurjchem-1635	38	40	h	h	NOUN
eurjchem-1635	38	41	to	to	ADP
eurjchem-1635	38	42	110	110	NUM
eurjchem-1635	38	43	°	°	NOUN
eurjchem-1635	38	44	c	c	NOUN
eurjchem-1635	38	45	,	,	PUNCT
eurjchem-1635	38	46	4	4	NUM
eurjchem-1635	38	47	h	h	NOUN
eurjchem-1635	38	48	;	;	PUNCT
eurjchem-1635	38	49	(	(	PUNCT
eurjchem-1635	38	50	b	b	X
eurjchem-1635	38	51	)	)	PUNCT
eurjchem-1635	38	52	benzyl	benzyl	NOUN
eurjchem-1635	38	53	bromide	bromide	NOUN
eurjchem-1635	38	54	,	,	PUNCT
eurjchem-1635	38	55	2,6‐lutidine	2,6‐lutidine	NUM
eurjchem-1635	38	56	,	,	PUNCT
eurjchem-1635	38	57	dmap	dmap	NOUN
eurjchem-1635	38	58	,	,	PUNCT
eurjchem-1635	38	59	acetone	acetone	NOUN
eurjchem-1635	38	60	,	,	PUNCT
eurjchem-1635	38	61	room	room	NOUN
eurjchem-1635	38	62	temperature	temperature	NOUN
eurjchem-1635	38	63	to	to	ADP
eurjchem-1635	38	64	80	80	NUM
eurjchem-1635	38	65	°	°	NOUN
eurjchem-1635	38	66	c	c	NOUN
eurjchem-1635	38	67	,	,	PUNCT
eurjchem-1635	38	68	1	1	NUM
eurjchem-1635	38	69	h	h	NOUN
eurjchem-1635	38	70	;	;	PUNCT
eurjchem-1635	38	71	(	(	PUNCT
eurjchem-1635	38	72	c	c	X
eurjchem-1635	38	73	)	)	PUNCT
eurjchem-1635	38	74	h2	h2	NOUN
eurjchem-1635	38	75	,	,	PUNCT
eurjchem-1635	38	76	raney	raney	PROPN
eurjchem-1635	38	77	ni	ni	PROPN
eurjchem-1635	38	78	,	,	PUNCT
eurjchem-1635	38	79	methanolic	methanolic	NOUN
eurjchem-1635	38	80	ammonia	ammonia	NOUN
eurjchem-1635	38	81	,	,	PUNCT
eurjchem-1635	38	82	room	room	NOUN
eurjchem-1635	38	83	temperature	temperature	NOUN
eurjchem-1635	38	84	;	;	PUNCT
eurjchem-1635	38	85	(	(	PUNCT
eurjchem-1635	38	86	d	d	X
eurjchem-1635	38	87	)	)	PUNCT
eurjchem-1635	38	88	substituted	substitute	VERB
eurjchem-1635	38	89	sulfonyl	sulfonyl	NOUN
eurjchem-1635	38	90	chlorides	chloride	NOUN
eurjchem-1635	38	91	,	,	PUNCT
eurjchem-1635	38	92	pyridine	pyridine	NOUN
eurjchem-1635	38	93	,	,	PUNCT
eurjchem-1635	38	94	dcm	dcm	PROPN
eurjchem-1635	38	95	,	,	PUNCT
eurjchem-1635	38	96	room	room	NOUN
eurjchem-1635	38	97	temperature	temperature	NOUN
eurjchem-1635	38	98	.	.	PUNCT
eurjchem-1635	39	1	r1	r1	PROPN
eurjchem-1635	39	2	=	=	PUNCT
eurjchem-1635	39	3	(	(	PUNCT
eurjchem-1635	39	4	a	a	DET
eurjchem-1635	39	5	)	)	PUNCT
eurjchem-1635	39	6	benzene	benzene	NOUN
eurjchem-1635	39	7	sulfonyl	sulfonyl	NOUN
eurjchem-1635	39	8	chloride	chloride	NOUN
eurjchem-1635	39	9	(	(	PUNCT
eurjchem-1635	39	10	b	b	NOUN
eurjchem-1635	39	11	)	)	PUNCT
eurjchem-1635	39	12	4‐methyl	4‐methyl	ADJ
eurjchem-1635	39	13	benzene	benzene	NOUN
eurjchem-1635	39	14	sulfonyl	sulfonyl	NOUN
eurjchem-1635	39	15	chloride	chloride	NOUN
eurjchem-1635	39	16	(	(	PUNCT
eurjchem-1635	39	17	c	c	NOUN
eurjchem-1635	39	18	)	)	PUNCT
eurjchem-1635	39	19	4‐chloro	4‐chloro	NUM
eurjchem-1635	39	20	benzene	benzene	NOUN
eurjchem-1635	39	21	sulfonyl	sulfonyl	NOUN
eurjchem-1635	39	22	chloride	chloride	NOUN
eurjchem-1635	39	23	(	(	PUNCT
eurjchem-1635	39	24	d	d	NOUN
eurjchem-1635	39	25	)	)	PUNCT
eurjchem-1635	39	26	4‐triflouromethyl	4‐triflouromethyl	PROPN
eurjchem-1635	39	27	benzene	benzene	NOUN
eurjchem-1635	39	28	sulfonyl	sulfonyl	NOUN
eurjchem-1635	39	29	chloride	chloride	NOUN
eurjchem-1635	39	30	(	(	PUNCT
eurjchem-1635	39	31	e	e	NOUN
eurjchem-1635	39	32	)	)	PUNCT
eurjchem-1635	39	33	methyl	methyl	NOUN
eurjchem-1635	39	34	sulfonyl	sulfonyl	NOUN
eurjchem-1635	39	35	chloride	chloride	NOUN
eurjchem-1635	39	36	.	.	PUNCT
eurjchem-1635	40	1	scheme	scheme	NOUN
eurjchem-1635	40	2	1	1	NUM
eurjchem-1635	40	3	reagents	reagent	NOUN
eurjchem-1635	40	4	and	and	CCONJ
eurjchem-1635	40	5	conditions	condition	NOUN
eurjchem-1635	40	6	:	:	PUNCT
eurjchem-1635	40	7	(	(	PUNCT
eurjchem-1635	40	8	a	a	X
eurjchem-1635	40	9	)	)	PUNCT
eurjchem-1635	40	10	2‐chloromethylacrylonitrile	2‐chloromethylacrylonitrile	NUM
eurjchem-1635	40	11	,	,	PUNCT
eurjchem-1635	40	12	cs2co3	cs2co3	ADJ
eurjchem-1635	40	13	,	,	PUNCT
eurjchem-1635	40	14	toluene	toluene	NOUN
eurjchem-1635	40	15	,	,	PUNCT
eurjchem-1635	40	16	60	60	NUM
eurjchem-1635	40	17	°	°	NOUN
eurjchem-1635	40	18	c	c	NOUN
eurjchem-1635	40	19	,	,	PUNCT
eurjchem-1635	40	20	0.5	0.5	NUM
eurjchem-1635	40	21	h	h	NOUN
eurjchem-1635	40	22	to	to	ADP
eurjchem-1635	40	23	110	110	NUM
eurjchem-1635	40	24	°	°	NOUN
eurjchem-1635	40	25	c	c	NOUN
eurjchem-1635	40	26	,	,	PUNCT
eurjchem-1635	40	27	4	4	NUM
eurjchem-1635	40	28	h	h	NOUN
eurjchem-1635	40	29	;	;	PUNCT
eurjchem-1635	40	30	(	(	PUNCT
eurjchem-1635	40	31	b	b	X
eurjchem-1635	40	32	)	)	PUNCT
eurjchem-1635	40	33	phenylmethanethiol	phenylmethanethiol	NOUN
eurjchem-1635	40	34	,	,	PUNCT
eurjchem-1635	40	35	naoh	naoh	NOUN
eurjchem-1635	40	36	,	,	PUNCT
eurjchem-1635	40	37	thf	thf	NOUN
eurjchem-1635	40	38	room	room	NOUN
eurjchem-1635	40	39	temperature	temperature	NOUN
eurjchem-1635	40	40	to	to	ADP
eurjchem-1635	40	41	80	80	NUM
eurjchem-1635	40	42	°	°	NOUN
eurjchem-1635	40	43	c	c	NOUN
eurjchem-1635	40	44	,	,	PUNCT
eurjchem-1635	40	45	1	1	NUM
eurjchem-1635	40	46	h	h	NOUN
eurjchem-1635	40	47	;	;	PUNCT
eurjchem-1635	40	48	(	(	PUNCT
eurjchem-1635	40	49	d	d	X
eurjchem-1635	40	50	)	)	PUNCT
eurjchem-1635	40	51	substituted	substitute	VERB
eurjchem-1635	40	52	sulfonyl	sulfonyl	NOUN
eurjchem-1635	40	53	chlorides	chloride	NOUN
eurjchem-1635	40	54	,	,	PUNCT
eurjchem-1635	40	55	pyridine	pyridine	NOUN
eurjchem-1635	40	56	,	,	PUNCT
eurjchem-1635	40	57	dcm	dcm	PROPN
eurjchem-1635	40	58	,	,	PUNCT
eurjchem-1635	40	59	room	room	NOUN
eurjchem-1635	40	60	temperature	temperature	NOUN
eurjchem-1635	40	61	.	.	PUNCT
eurjchem-1635	41	1	r1	r1	PROPN
eurjchem-1635	41	2	=	=	PUNCT
eurjchem-1635	41	3	(	(	PUNCT
eurjchem-1635	41	4	a	a	DET
eurjchem-1635	41	5	)	)	PUNCT
eurjchem-1635	41	6	benzene	benzene	NOUN
eurjchem-1635	41	7	sulfonyl	sulfonyl	NOUN
eurjchem-1635	41	8	chloride	chloride	NOUN
eurjchem-1635	41	9	(	(	PUNCT
eurjchem-1635	41	10	b	b	NOUN
eurjchem-1635	41	11	)	)	PUNCT
eurjchem-1635	41	12	4‐methyl	4‐methyl	ADJ
eurjchem-1635	41	13	benzene	benzene	NOUN
eurjchem-1635	41	14	sulfonyl	sulfonyl	NOUN
eurjchem-1635	41	15	chloride	chloride	NOUN
eurjchem-1635	41	16	(	(	PUNCT
eurjchem-1635	41	17	c	c	NOUN
eurjchem-1635	41	18	)	)	PUNCT
eurjchem-1635	41	19	4‐	4‐	PROPN
eurjchem-1635	41	20	chloro	chloro	NOUN
eurjchem-1635	41	21	benzene	benzene	NOUN
eurjchem-1635	41	22	sulfonyl	sulfonyl	NOUN
eurjchem-1635	41	23	chloride	chloride	NOUN
eurjchem-1635	41	24	(	(	PUNCT
eurjchem-1635	41	25	d	d	NOUN
eurjchem-1635	41	26	)	)	PUNCT
eurjchem-1635	41	27	4‐triflouromethyl	4‐triflouromethyl	PROPN
eurjchem-1635	41	28	benzene	benzene	NOUN
eurjchem-1635	41	29	sulfonyl	sulfonyl	NOUN
eurjchem-1635	41	30	chloride	chloride	NOUN
eurjchem-1635	41	31	(	(	PUNCT
eurjchem-1635	41	32	e	e	NOUN
eurjchem-1635	41	33	)	)	PUNCT
eurjchem-1635	41	34	methyl	methyl	NOUN
eurjchem-1635	41	35	sulfonyl	sulfonyl	NOUN
eurjchem-1635	41	36	chloride	chloride	NOUN
eurjchem-1635	41	37	.	.	PUNCT
eurjchem-1635	42	1	scheme	scheme	NOUN
eurjchem-1635	42	2	2	2	NUM
eurjchem-1635	42	3	all	all	DET
eurjchem-1635	42	4	chemicals	chemical	NOUN
eurjchem-1635	42	5	,	,	PUNCT
eurjchem-1635	42	6	unless	unless	SCONJ
eurjchem-1635	42	7	otherwise	otherwise	ADV
eurjchem-1635	42	8	specified	specify	VERB
eurjchem-1635	42	9	,	,	PUNCT
eurjchem-1635	42	10	were	be	AUX
eurjchem-1635	42	11	purchased	purchase	VERB
eurjchem-1635	42	12	from	from	ADP
eurjchem-1635	42	13	commercial	commercial	ADJ
eurjchem-1635	42	14	sources	source	NOUN
eurjchem-1635	42	15	and	and	CCONJ
eurjchem-1635	42	16	were	be	AUX
eurjchem-1635	42	17	used	use	VERB
eurjchem-1635	42	18	without	without	ADP
eurjchem-1635	42	19	further	further	ADJ
eurjchem-1635	42	20	purification	purification	NOUN
eurjchem-1635	42	21	.	.	PUNCT
eurjchem-1635	43	1	the	the	DET
eurjchem-1635	43	2	major	major	ADJ
eurjchem-1635	43	3	chemicals	chemical	NOUN
eurjchem-1635	43	4	were	be	AUX
eurjchem-1635	43	5	purchased	purchase	VERB
eurjchem-1635	43	6	from	from	ADP
eurjchem-1635	43	7	sigma	sigma	PROPN
eurjchem-1635	43	8	aldrich	aldrich	PROPN
eurjchem-1635	43	9	and	and	CCONJ
eurjchem-1635	43	10	avra	avra	ADJ
eurjchem-1635	43	11	labs	lab	NOUN
eurjchem-1635	43	12	.	.	PUNCT
eurjchem-1635	44	1	the	the	DET
eurjchem-1635	44	2	development	development	NOUN
eurjchem-1635	44	3	of	of	ADP
eurjchem-1635	44	4	reactions	reaction	NOUN
eurjchem-1635	44	5	was	be	AUX
eurjchem-1635	44	6	monitored	monitor	VERB
eurjchem-1635	44	7	by	by	ADP
eurjchem-1635	44	8	thin	thin	ADJ
eurjchem-1635	44	9	layer	layer	NOUN
eurjchem-1635	44	10	chromatography	chromatography	NOUN
eurjchem-1635	44	11	(	(	PUNCT
eurjchem-1635	44	12	tlc	tlc	NOUN
eurjchem-1635	44	13	)	)	PUNCT
eurjchem-1635	44	14	analysis	analysis	NOUN
eurjchem-1635	44	15	on	on	ADP
eurjchem-1635	44	16	merck	merck	NOUN
eurjchem-1635	44	17	pre‐coated	pre‐coate	VERB
eurjchem-1635	44	18	silica	silica	NOUN
eurjchem-1635	44	19	gel	gel	NOUN
eurjchem-1635	44	20	60	60	NUM
eurjchem-1635	44	21	f254	f254	PROPN
eurjchem-1635	44	22	aluminum	aluminum	NOUN
eurjchem-1635	44	23	sheets	sheet	NOUN
eurjchem-1635	44	24	,	,	PUNCT
eurjchem-1635	44	25	visualized	visualize	VERB
eurjchem-1635	44	26	by	by	ADP
eurjchem-1635	44	27	uv	uv	NOUN
eurjchem-1635	44	28	light	light	NOUN
eurjchem-1635	44	29	.	.	PUNCT
eurjchem-1635	45	1	all	all	DET
eurjchem-1635	45	2	reactions	reaction	NOUN
eurjchem-1635	45	3	were	be	AUX
eurjchem-1635	45	4	carried	carry	VERB
eurjchem-1635	45	5	out	out	ADP
eurjchem-1635	45	6	under	under	ADP
eurjchem-1635	45	7	argon	argon	NOUN
eurjchem-1635	45	8	inert	inert	NOUN
eurjchem-1635	45	9	atmosphere	atmosphere	PROPN
eurjchem-1635	45	10	.	.	PUNCT
eurjchem-1635	46	1	melting	melt	VERB
eurjchem-1635	46	2	points	point	NOUN
eurjchem-1635	46	3	were	be	AUX
eurjchem-1635	46	4	recorded	record	VERB
eurjchem-1635	46	5	on	on	ADP
eurjchem-1635	46	6	srs	srs	PROPN
eurjchem-1635	46	7	optimelt	optimelt	PROPN
eurjchem-1635	46	8	,	,	PUNCT
eurjchem-1635	46	9	melting	melt	VERB
eurjchem-1635	46	10	point	point	NOUN
eurjchem-1635	46	11	apparatus	apparatus	NOUN
eurjchem-1635	46	12	and	and	CCONJ
eurjchem-1635	46	13	are	be	AUX
eurjchem-1635	46	14	uncorrected	uncorrecte	VERB
eurjchem-1635	46	15	.	.	PUNCT
eurjchem-1635	47	1	the	the	DET
eurjchem-1635	47	2	purity	purity	NOUN
eurjchem-1635	47	3	of	of	ADP
eurjchem-1635	47	4	intermediates	intermediate	NOUN
eurjchem-1635	47	5	was	be	AUX
eurjchem-1635	47	6	assessed	assess	VERB
eurjchem-1635	47	7	by	by	ADP
eurjchem-1635	47	8	tlc	tlc	PROPN
eurjchem-1635	47	9	,	,	PUNCT
eurjchem-1635	47	10	nmr	nmr	NOUN
eurjchem-1635	47	11	,	,	PUNCT
eurjchem-1635	47	12	and	and	CCONJ
eurjchem-1635	47	13	lc‐ms	lc‐ms	AUX
eurjchem-1635	47	14	.	.	PUNCT
eurjchem-1635	48	1	the	the	DET
eurjchem-1635	48	2	purities	purity	NOUN
eurjchem-1635	48	3	of	of	ADP
eurjchem-1635	48	4	final	final	ADJ
eurjchem-1635	48	5	compounds	compound	NOUN
eurjchem-1635	48	6	were	be	AUX
eurjchem-1635	48	7	assessed	assess	VERB
eurjchem-1635	48	8	by	by	ADP
eurjchem-1635	48	9	nmr	nmr	NOUN
eurjchem-1635	48	10	,	,	PUNCT
eurjchem-1635	48	11	lc‐ms	lc‐ms	NOUN
eurjchem-1635	48	12	and	and	CCONJ
eurjchem-1635	48	13	hplc	hplc	PROPN
eurjchem-1635	48	14	and	and	CCONJ
eurjchem-1635	48	15	all	all	DET
eurjchem-1635	48	16	structures	structure	NOUN
eurjchem-1635	48	17	are	be	AUX
eurjchem-1635	48	18	consistent	consistent	ADJ
eurjchem-1635	48	19	with	with	ADP
eurjchem-1635	48	20	proposed	propose	VERB
eurjchem-1635	48	21	struc‐	struc‐	PROPN
eurjchem-1635	48	22	tures	ture	NOUN
eurjchem-1635	48	23	characterization	characterization	NOUN
eurjchem-1635	48	24	.	.	PUNCT
eurjchem-1635	49	1	the	the	DET
eurjchem-1635	49	2	1h	1h	NUM
eurjchem-1635	49	3	nmr	nmr	NOUN
eurjchem-1635	49	4	spectra	spectra	NOUN
eurjchem-1635	49	5	were	be	AUX
eurjchem-1635	49	6	recorded	record	VERB
eurjchem-1635	49	7	on	on	ADP
eurjchem-1635	49	8	varian	varian	PROPN
eurjchem-1635	49	9	nmr	nmr	NOUN
eurjchem-1635	49	10	(	(	PUNCT
eurjchem-1635	49	11	400	400	NUM
eurjchem-1635	49	12	mhz	mhz	NOUN
eurjchem-1635	49	13	)	)	PUNCT
eurjchem-1635	49	14	spectrometer	spectrometer	NOUN
eurjchem-1635	49	15	.	.	PUNCT
eurjchem-1635	50	1	the	the	DET
eurjchem-1635	50	2	13c	13c	NUM
eurjchem-1635	50	3	nmr	nmr	NOUN
eurjchem-1635	50	4	spectra	spectra	NOUN
eurjchem-1635	50	5	were	be	AUX
eurjchem-1635	50	6	recorded	record	VERB
eurjchem-1635	50	7	on	on	ADP
eurjchem-1635	50	8	varian	varian	PROPN
eurjchem-1635	50	9	nmr	nmr	NOUN
eurjchem-1635	50	10	(	(	PUNCT
eurjchem-1635	50	11	100	100	NUM
eurjchem-1635	50	12	mhz	mhz	NOUN
eurjchem-1635	50	13	)	)	PUNCT
eurjchem-1635	50	14	spectrometer	spectrometer	NOUN
eurjchem-1635	50	15	.	.	PUNCT
eurjchem-1635	51	1	the	the	DET
eurjchem-1635	51	2	chemical	chemical	ADJ
eurjchem-1635	51	3	shifts	shift	NOUN
eurjchem-1635	51	4	are	be	AUX
eurjchem-1635	51	5	reported	report	VERB
eurjchem-1635	51	6	as	as	ADP
eurjchem-1635	51	7	nmr	nmr	NOUN
eurjchem-1635	51	8	spectra	spectra	ADJ
eurjchem-1635	51	9	δppm	δppm	ADJ
eurjchem-1635	51	10	units	unit	NOUN
eurjchem-1635	51	11	.	.	PUNCT
eurjchem-1635	52	1	the	the	DET
eurjchem-1635	52	2	following	follow	VERB
eurjchem-1635	52	3	abbreviations	abbreviation	NOUN
eurjchem-1635	52	4	are	be	AUX
eurjchem-1635	52	5	used	use	VERB
eurjchem-1635	52	6	;	;	PUNCT
eurjchem-1635	52	7	singlet	singlet	NOUN
eurjchem-1635	52	8	(	(	PUNCT
eurjchem-1635	52	9	s	s	NOUN
eurjchem-1635	52	10	)	)	PUNCT
eurjchem-1635	52	11	,	,	PUNCT
eurjchem-1635	52	12	doublet	doublet	NOUN
eurjchem-1635	52	13	(	(	PUNCT
eurjchem-1635	52	14	d	d	NOUN
eurjchem-1635	52	15	)	)	PUNCT
eurjchem-1635	52	16	,	,	PUNCT
eurjchem-1635	52	17	triplet	triplet	NOUN
eurjchem-1635	52	18	(	(	PUNCT
eurjchem-1635	52	19	t	t	NOUN
eurjchem-1635	52	20	)	)	PUNCT
eurjchem-1635	52	21	,	,	PUNCT
eurjchem-1635	52	22	quartet	quartet	NOUN
eurjchem-1635	52	23	(	(	PUNCT
eurjchem-1635	52	24	q	q	NOUN
eurjchem-1635	52	25	)	)	PUNCT
eurjchem-1635	52	26	,	,	PUNCT
eurjchem-1635	52	27	multiplet	multiplet	NOUN
eurjchem-1635	52	28	(	(	PUNCT
eurjchem-1635	52	29	m	m	NOUN
eurjchem-1635	52	30	)	)	PUNCT
eurjchem-1635	52	31	and	and	CCONJ
eurjchem-1635	52	32	broad	broad	ADJ
eurjchem-1635	52	33	(	(	PUNCT
eurjchem-1635	52	34	br	br	NOUN
eurjchem-1635	52	35	)	)	PUNCT
eurjchem-1635	52	36	.	.	PUNCT
eurjchem-1635	53	1	mass	mass	PROPN
eurjchem-1635	53	2	spectra	spectra	PROPN
eurjchem-1635	53	3	were	be	AUX
eurjchem-1635	53	4	taken	take	VERB
eurjchem-1635	53	5	using	use	VERB
eurjchem-1635	53	6	varian	varian	NOUN
eurjchem-1635	53	7	vg	vg	ADP
eurjchem-1635	53	8	7070	7070	NUM
eurjchem-1635	53	9	spectrometer	spectrometer	NOUN
eurjchem-1635	53	10	at	at	ADP
eurjchem-1635	53	11	nominal	nominal	ADJ
eurjchem-1635	53	12	5000	5000	NUM
eurjchem-1635	53	13	resolution	resolution	NOUN
eurjchem-1635	53	14	.	.	PUNCT
eurjchem-1635	54	1	purity	purity	NOUN
eurjchem-1635	54	2	of	of	ADP
eurjchem-1635	54	3	final	final	ADJ
eurjchem-1635	54	4	compounds	compound	NOUN
eurjchem-1635	54	5	were	be	AUX
eurjchem-1635	54	6	determined	determine	VERB
eurjchem-1635	54	7	to	to	PART
eurjchem-1635	54	8	be	be	AUX
eurjchem-1635	54	9	>	>	X
eurjchem-1635	54	10	95	95	NUM
eurjchem-1635	54	11	%	%	NOUN
eurjchem-1635	54	12	by	by	ADP
eurjchem-1635	54	13	hplc	hplc	NOUN
eurjchem-1635	54	14	on	on	ADP
eurjchem-1635	54	15	an	an	DET
eurjchem-1635	54	16	alltech	alltech	ADJ
eurjchem-1635	54	17	alltima	alltima	NOUN
eurjchem-1635	54	18	c18	c18	NOUN
eurjchem-1635	54	19	column	column	NOUN
eurjchem-1635	54	20	(	(	PUNCT
eurjchem-1635	54	21	3.2	3.2	NUM
eurjchem-1635	54	22	×	×	NOUN
eurjchem-1635	54	23	150	150	NUM
eurjchem-1635	54	24	mm	mm	NOUN
eurjchem-1635	54	25	,	,	PUNCT
eurjchem-1635	54	26	5	5	NUM
eurjchem-1635	54	27	µm	µm	NOUN
eurjchem-1635	54	28	)	)	PUNCT
eurjchem-1635	54	29	eluting	eluting	NOUN
eurjchem-1635	54	30	with	with	ADP
eurjchem-1635	54	31	5‐80	5‐80	NUM
eurjchem-1635	54	32	%	%	NOUN
eurjchem-1635	54	33	aceto‐	aceto‐	PUNCT
eurjchem-1635	54	34	nitrile/45	nitrile/45	VERB
eurjchem-1635	54	35	nm	nm	DET
eurjchem-1635	54	36	sodium	sodium	NOUN
eurjchem-1635	54	37	bicarbonate	bicarbonate	NOUN
eurjchem-1635	54	38	.	.	PUNCT
eurjchem-1635	55	1	2.2	2.2	NUM
eurjchem-1635	55	2	.	.	PUNCT
eurjchem-1635	55	3	synthesis	synthesis	NOUN
eurjchem-1635	55	4	2.2.1	2.2.1	NUM
eurjchem-1635	55	5	.	.	PUNCT
eurjchem-1635	55	6	synthesis	synthesis	NOUN
eurjchem-1635	55	7	of	of	ADP
eurjchem-1635	55	8	3,4‐dihydro‐2h‐benzo[b][1,4]oxazine‐2‐	3,4‐dihydro‐2h‐benzo[b][1,4]oxazine‐2‐	NUM
eurjchem-1635	55	9	carbonitrile	carbonitrile	ADJ
eurjchem-1635	55	10	(	(	PUNCT
eurjchem-1635	55	11	1	1	NUM
eurjchem-1635	55	12	)	)	PUNCT
eurjchem-1635	55	13	to	to	ADP
eurjchem-1635	55	14	a	a	DET
eurjchem-1635	55	15	stirred	stir	VERB
eurjchem-1635	55	16	solution	solution	NOUN
eurjchem-1635	55	17	of	of	ADP
eurjchem-1635	55	18	2‐aminophenol	2‐aminophenol	NUM
eurjchem-1635	55	19	(	(	PUNCT
eurjchem-1635	55	20	5	5	NUM
eurjchem-1635	55	21	g	g	NOUN
eurjchem-1635	55	22	,	,	PUNCT
eurjchem-1635	55	23	45.8	45.8	NUM
eurjchem-1635	55	24	mmol	mmol	NOUN
eurjchem-1635	55	25	)	)	PUNCT
eurjchem-1635	55	26	was	be	AUX
eurjchem-1635	55	27	dissolved	dissolve	VERB
eurjchem-1635	55	28	in	in	ADP
eurjchem-1635	55	29	toluene	toluene	NOUN
eurjchem-1635	55	30	(	(	PUNCT
eurjchem-1635	55	31	50	50	NUM
eurjchem-1635	55	32	ml	ml	NOUN
eurjchem-1635	55	33	)	)	PUNCT
eurjchem-1635	55	34	then	then	ADV
eurjchem-1635	55	35	added	add	VERB
eurjchem-1635	55	36	cesium	cesium	NOUN
eurjchem-1635	55	37	carbonate	carbonate	NOUN
eurjchem-1635	55	38	(	(	PUNCT
eurjchem-1635	55	39	17.9	17.9	NUM
eurjchem-1635	55	40	g	g	NOUN
eurjchem-1635	55	41	,	,	PUNCT
eurjchem-1635	55	42	55.0	55.0	NUM
eurjchem-1635	55	43	mmol	mmol	NOUN
eurjchem-1635	55	44	)	)	PUNCT
eurjchem-1635	55	45	.	.	PUNCT
eurjchem-1635	56	1	stirred	stir	VERB
eurjchem-1635	56	2	reaction	reaction	NOUN
eurjchem-1635	56	3	mixture	mixture	NOUN
eurjchem-1635	56	4	at	at	ADP
eurjchem-1635	56	5	60	60	NUM
eurjchem-1635	56	6	°	°	ADP
eurjchem-1635	56	7	c	c	NOUN
eurjchem-1635	56	8	for	for	ADP
eurjchem-1635	56	9	0.5	0.5	NUM
eurjchem-1635	56	10	h	h	NOUN
eurjchem-1635	56	11	then	then	ADV
eurjchem-1635	56	12	added	add	VERB
eurjchem-1635	56	13	2‐chloroacrylonitrile	2‐chloroacrylonitrile	NUM
eurjchem-1635	56	14	(	(	PUNCT
eurjchem-1635	56	15	4.79	4.79	NUM
eurjchem-1635	56	16	g	g	NOUN
eurjchem-1635	56	17	,	,	PUNCT
eurjchem-1635	56	18	55.0	55.0	NUM
eurjchem-1635	56	19	mmol	mmol	NOUN
eurjchem-1635	56	20	)	)	PUNCT
eurjchem-1635	56	21	and	and	CCONJ
eurjchem-1635	56	22	heat	heat	NOUN
eurjchem-1635	56	23	reaction	reaction	NOUN
eurjchem-1635	56	24	mixture	mixture	NOUN
eurjchem-1635	56	25	at	at	ADP
eurjchem-1635	56	26	110	110	NUM
eurjchem-1635	56	27	°	°	NOUN
eurjchem-1635	56	28	c	c	NOUN
eurjchem-1635	56	29	for	for	ADP
eurjchem-1635	56	30	4	4	NUM
eurjchem-1635	56	31	h.	h.	NOUN
eurjchem-1635	56	32	progress	progress	NOUN
eurjchem-1635	56	33	of	of	ADP
eurjchem-1635	56	34	reaction	reaction	NOUN
eurjchem-1635	56	35	was	be	AUX
eurjchem-1635	56	36	monitored	monitor	VERB
eurjchem-1635	56	37	by	by	ADP
eurjchem-1635	56	38	tlc	tlc	PROPN
eurjchem-1635	56	39	.	.	PUNCT
eurjchem-1635	57	1	after	after	ADP
eurjchem-1635	57	2	completion	completion	NOUN
eurjchem-1635	57	3	the	the	DET
eurjchem-1635	57	4	reaction	reaction	NOUN
eurjchem-1635	57	5	,	,	PUNCT
eurjchem-1635	57	6	we	we	PRON
eurjchem-1635	57	7	evaporated	evaporate	VERB
eurjchem-1635	57	8	reaction	reaction	NOUN
eurjchem-1635	57	9	mixture	mixture	NOUN
eurjchem-1635	57	10	under	under	ADP
eurjchem-1635	57	11	reduced	reduce	VERB
eurjchem-1635	57	12	pressure	pressure	NOUN
eurjchem-1635	57	13	to	to	PART
eurjchem-1635	57	14	obtain	obtain	VERB
eurjchem-1635	57	15	crude	crude	ADJ
eurjchem-1635	57	16	yellow	yellow	ADJ
eurjchem-1635	57	17	gummy	gummy	ADJ
eurjchem-1635	57	18	mass	mass	NOUN
eurjchem-1635	57	19	.	.	PUNCT
eurjchem-1635	58	1	added	add	VERB
eurjchem-1635	58	2	h2o	h2o	PROPN
eurjchem-1635	58	3	(	(	PUNCT
eurjchem-1635	58	4	50	50	NUM
eurjchem-1635	58	5	ml	ml	NOUN
eurjchem-1635	58	6	)	)	PUNCT
eurjchem-1635	58	7	and	and	CCONJ
eurjchem-1635	58	8	extracted	extract	VERB
eurjchem-1635	58	9	it	it	PRON
eurjchem-1635	58	10	with	with	ADP
eurjchem-1635	58	11	ethyl	ethyl	PROPN
eurjchem-1635	58	12	acetate	acetate	PROPN
eurjchem-1635	58	13	(	(	PUNCT
eurjchem-1635	58	14	etoac	etoac	ADJ
eurjchem-1635	58	15	)	)	PUNCT
eurjchem-1635	58	16	(	(	PUNCT
eurjchem-1635	58	17	2	2	NUM
eurjchem-1635	58	18	×	×	NOUN
eurjchem-1635	58	19	50	50	NUM
eurjchem-1635	58	20	ml	ml	NOUN
eurjchem-1635	58	21	)	)	PUNCT
eurjchem-1635	58	22	.	.	PUNCT
eurjchem-1635	59	1	the	the	DET
eurjchem-1635	59	2	organic	organic	ADJ
eurjchem-1635	59	3	layer	layer	NOUN
eurjchem-1635	59	4	was	be	AUX
eurjchem-1635	59	5	separated	separate	VERB
eurjchem-1635	59	6	,	,	PUNCT
eurjchem-1635	59	7	washed	wash	VERB
eurjchem-1635	59	8	with	with	ADP
eurjchem-1635	59	9	h2o	h2o	PROPN
eurjchem-1635	59	10	(	(	PUNCT
eurjchem-1635	59	11	25	25	NUM
eurjchem-1635	59	12	ml	ml	NOUN
eurjchem-1635	59	13	)	)	PUNCT
eurjchem-1635	59	14	and	and	CCONJ
eurjchem-1635	59	15	brine	brine	NOUN
eurjchem-1635	59	16	(	(	PUNCT
eurjchem-1635	59	17	25	25	NUM
eurjchem-1635	59	18	ml	ml	NOUN
eurjchem-1635	59	19	)	)	PUNCT
eurjchem-1635	59	20	,	,	PUNCT
eurjchem-1635	59	21	dried	dry	VERB
eurjchem-1635	59	22	over	over	ADP
eurjchem-1635	59	23	anhydrous	anhydrous	ADJ
eurjchem-1635	59	24	na2so4	na2so4	NOUN
eurjchem-1635	59	25	and	and	CCONJ
eurjchem-1635	59	26	concentrated	concentrate	VERB
eurjchem-1635	59	27	in	in	ADP
eurjchem-1635	59	28	vacuum	vacuum	NOUN
eurjchem-1635	59	29	.	.	PUNCT
eurjchem-1635	60	1	purification	purification	NOUN
eurjchem-1635	60	2	of	of	ADP
eurjchem-1635	60	3	crude	crude	NOUN
eurjchem-1635	60	4	done	do	VERB
eurjchem-1635	60	5	by	by	ADP
eurjchem-1635	60	6	silica	silica	NOUN
eurjchem-1635	60	7	gel	gel	NOUN
eurjchem-1635	60	8	(	(	PUNCT
eurjchem-1635	60	9	100‐200	100‐200	NUM
eurjchem-1635	60	10	mesh	mesh	NOUN
eurjchem-1635	60	11	)	)	PUNCT
eurjchem-1635	60	12	column	column	NOUN
eurjchem-1635	60	13	chromatography	chromatography	NOUN
eurjchem-1635	60	14	by	by	ADP
eurjchem-1635	60	15	using	use	VERB
eurjchem-1635	60	16	etoac	etoac	ADJ
eurjchem-1635	60	17	:	:	PUNCT
eurjchem-1635	60	18	hexane	hexane	NOUN
eurjchem-1635	60	19	(	(	PUNCT
eurjchem-1635	60	20	10:90	10:90	NUM
eurjchem-1635	60	21	,	,	PUNCT
eurjchem-1635	60	22	v	v	NOUN
eurjchem-1635	60	23	:	:	SYM
eurjchem-1635	60	24	v	v	NOUN
eurjchem-1635	60	25	)	)	PUNCT
eurjchem-1635	60	26	to	to	PART
eurjchem-1635	60	27	obtain	obtain	VERB
eurjchem-1635	60	28	3,4‐dihydro‐2h‐benzo[b][1,4]oxazine‐2‐carbo‐	3,4‐dihydro‐2h‐benzo[b][1,4]oxazine‐2‐carbo‐	NUM
eurjchem-1635	60	29	nitrile	nitrile	NOUN
eurjchem-1635	60	30	(	(	PUNCT
eurjchem-1635	60	31	1	1	NUM
eurjchem-1635	60	32	)	)	PUNCT
eurjchem-1635	60	33	(	(	PUNCT
eurjchem-1635	60	34	scheme	scheme	NOUN
eurjchem-1635	60	35	1	1	NUM
eurjchem-1635	60	36	)	)	PUNCT
eurjchem-1635	60	37	.	.	PUNCT
eurjchem-1635	61	1	color	color	NOUN
eurjchem-1635	61	2	:	:	PUNCT
eurjchem-1635	61	3	yellow	yellow	ADJ
eurjchem-1635	61	4	solid	solid	ADJ
eurjchem-1635	61	5	.	.	PUNCT
eurjchem-1635	62	1	yield	yield	NOUN
eurjchem-1635	62	2	:	:	PUNCT
eurjchem-1635	62	3	6.66	6.66	NUM
eurjchem-1635	62	4	g	g	NOUN
eurjchem-1635	62	5	,	,	PUNCT
eurjchem-1635	62	6	90	90	NUM
eurjchem-1635	62	7	%	%	NOUN
eurjchem-1635	62	8	.	.	PUNCT
eurjchem-1635	63	1	ms	ms	NOUN
eurjchem-1635	63	2	(	(	PUNCT
eurjchem-1635	63	3	esi	esi	PROPN
eurjchem-1635	63	4	,	,	PUNCT
eurjchem-1635	63	5	m	m	PROPN
eurjchem-1635	63	6	/	/	SYM
eurjchem-1635	63	7	z	z	NOUN
eurjchem-1635	63	8	):	):	PUNCT
eurjchem-1635	63	9	161	161	NUM
eurjchem-1635	63	10	[	[	X
eurjchem-1635	63	11	m+h]+	m+h]+	X
eurjchem-1635	63	12	.	.	PUNCT
eurjchem-1635	64	1	1h	1h	NUM
eurjchem-1635	64	2	nmr	nmr	NOUN
eurjchem-1635	64	3	(	(	PUNCT
eurjchem-1635	64	4	400	400	NUM
eurjchem-1635	64	5	mhz	mhz	NOUN
eurjchem-1635	64	6	,	,	PUNCT
eurjchem-1635	64	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	64	8	,	,	PUNCT
eurjchem-1635	64	9	δ	δ	PROPN
eurjchem-1635	64	10	,	,	PUNCT
eurjchem-1635	64	11	ppm	ppm	NUM
eurjchem-1635	64	12	):	):	PUNCT
eurjchem-1635	64	13	3.42	3.42	NUM
eurjchem-1635	64	14	(	(	PUNCT
eurjchem-1635	64	15	dd	dd	PROPN
eurjchem-1635	64	16	,	,	PUNCT
eurjchem-1635	64	17	1h	1h	NUM
eurjchem-1635	64	18	,	,	PUNCT
eurjchem-1635	64	19	j	j	PROPN
eurjchem-1635	64	20	=	=	PROPN
eurjchem-1635	64	21	12.8	12.8	NUM
eurjchem-1635	64	22	,	,	PUNCT
eurjchem-1635	64	23	3.8	3.8	NUM
eurjchem-1635	64	24	hz	hz	NOUN
eurjchem-1635	64	25	,	,	PUNCT
eurjchem-1635	64	26	nh‐ch2	nh‐ch2	ADJ
eurjchem-1635	64	27	)	)	PUNCT
eurjchem-1635	64	28	,	,	PUNCT
eurjchem-1635	64	29	3.58	3.58	NUM
eurjchem-1635	64	30	(	(	PUNCT
eurjchem-1635	64	31	dd	dd	PROPN
eurjchem-1635	64	32	,	,	PUNCT
eurjchem-1635	64	33	1h	1h	NUM
eurjchem-1635	64	34	,	,	PUNCT
eurjchem-1635	64	35	j	j	PROPN
eurjchem-1635	64	36	=	=	PROPN
eurjchem-1635	64	37	12.4	12.4	NUM
eurjchem-1635	64	38	,	,	PUNCT
eurjchem-1635	64	39	3.6	3.6	NUM
eurjchem-1635	64	40	hz	hz	NOUN
eurjchem-1635	64	41	,	,	PUNCT
eurjchem-1635	64	42	nh‐ch2	nh‐ch2	ADJ
eurjchem-1635	64	43	)	)	PUNCT
eurjchem-1635	64	44	,	,	PUNCT
eurjchem-1635	64	45	5.57	5.57	NUM
eurjchem-1635	64	46	(	(	PUNCT
eurjchem-1635	64	47	s	s	PROPN
eurjchem-1635	64	48	,	,	PUNCT
eurjchem-1635	64	49	1h	1h	NUM
eurjchem-1635	64	50	,	,	PUNCT
eurjchem-1635	64	51	cn‐ch	cn‐ch	NUM
eurjchem-1635	64	52	)	)	PUNCT
eurjchem-1635	64	53	,	,	PUNCT
eurjchem-1635	64	54	6.19	6.19	NUM
eurjchem-1635	64	55	(	(	PUNCT
eurjchem-1635	64	56	s	s	PROPN
eurjchem-1635	64	57	,	,	PUNCT
eurjchem-1635	64	58	1h	1h	NUM
eurjchem-1635	64	59	,	,	PUNCT
eurjchem-1635	64	60	nh	nh	PROPN
eurjchem-1635	64	61	)	)	PUNCT
eurjchem-1635	64	62	,	,	PUNCT
eurjchem-1635	64	63	6.58	6.58	NUM
eurjchem-1635	64	64	(	(	PUNCT
eurjchem-1635	64	65	q	q	NOUN
eurjchem-1635	64	66	,	,	PUNCT
eurjchem-1635	64	67	1h	1h	NUM
eurjchem-1635	64	68	,	,	PUNCT
eurjchem-1635	64	69	ar‐h	ar‐h	NOUN
eurjchem-1635	64	70	)	)	PUNCT
eurjchem-1635	64	71	,	,	PUNCT
eurjchem-1635	64	72	6.64	6.64	NUM
eurjchem-1635	64	73	(	(	PUNCT
eurjchem-1635	64	74	d	d	PROPN
eurjchem-1635	64	75	,	,	PUNCT
eurjchem-1635	64	76	1h	1h	NUM
eurjchem-1635	64	77	,	,	PUNCT
eurjchem-1635	64	78	j	j	PROPN
eurjchem-1635	64	79	=	=	PROPN
eurjchem-1635	64	80	8.82	8.82	NUM
eurjchem-1635	64	81	hz	hz	NOUN
eurjchem-1635	64	82	,	,	PUNCT
eurjchem-1635	64	83	ar‐h	ar‐h	PROPN
eurjchem-1635	64	84	)	)	PUNCT
eurjchem-1635	64	85	,	,	PUNCT
eurjchem-1635	64	86	6.78	6.78	NUM
eurjchem-1635	64	87	(	(	PUNCT
eurjchem-1635	64	88	q	q	NOUN
eurjchem-1635	64	89	,	,	PUNCT
eurjchem-1635	64	90	2h	2h	NUM
eurjchem-1635	64	91	,	,	PUNCT
eurjchem-1635	64	92	ar‐h	ar‐h	NOUN
eurjchem-1635	64	93	)	)	PUNCT
eurjchem-1635	64	94	.	.	PUNCT
eurjchem-1635	65	1	1h	1h	NUM
eurjchem-1635	65	2	nmr	nmr	NOUN
eurjchem-1635	65	3	of	of	ADP
eurjchem-1635	65	4	undesired	undesired	ADJ
eurjchem-1635	65	5	1a	1a	NOUN
eurjchem-1635	65	6	:	:	PUNCT
eurjchem-1635	65	7	6.8‐6.78	6.8‐6.78	NUM
eurjchem-1635	65	8	(	(	PUNCT
eurjchem-1635	65	9	m	m	PROPN
eurjchem-1635	65	10	,	,	PUNCT
eurjchem-1635	65	11	2h	2h	NUM
eurjchem-1635	65	12	)	)	PUNCT
eurjchem-1635	65	13	,	,	PUNCT
eurjchem-1635	65	14	6.61‐6.58	6.61‐6.58	NUM
eurjchem-1635	65	15	(	(	PUNCT
eurjchem-1635	65	16	m	m	PROPN
eurjchem-1635	65	17	,	,	PUNCT
eurjchem-1635	65	18	2h	2h	NUM
eurjchem-1635	65	19	)	)	PUNCT
eurjchem-1635	65	20	,	,	PUNCT
eurjchem-1635	65	21	5.61	5.61	NUM
eurjchem-1635	65	22	(	(	PUNCT
eurjchem-1635	65	23	m	m	PROPN
eurjchem-1635	65	24	,	,	PUNCT
eurjchem-1635	65	25	1h	1h	NUM
eurjchem-1635	65	26	)	)	PUNCT
eurjchem-1635	65	27	,	,	PUNCT
eurjchem-1635	65	28	4.38‐4.29	4.38‐4.29	NUM
eurjchem-1635	65	29	(	(	PUNCT
eurjchem-1635	65	30	q	q	NOUN
eurjchem-1635	65	31	,	,	PUNCT
eurjchem-1635	65	32	2h	2h	NUM
eurjchem-1635	65	33	)	)	PUNCT
eurjchem-1635	65	34	,	,	PUNCT
eurjchem-1635	65	35	4.01	4.01	NUM
eurjchem-1635	65	36	(	(	PUNCT
eurjchem-1635	65	37	br	br	PROPN
eurjchem-1635	65	38	,	,	PUNCT
eurjchem-1635	65	39	1h	1h	NUM
eurjchem-1635	65	40	,	,	PUNCT
eurjchem-1635	65	41	nh	nh	PROPN
eurjchem-1635	65	42	)	)	PUNCT
eurjchem-1635	65	43	.	.	PUNCT
eurjchem-1635	66	1	2.2.2	2.2.2	X
eurjchem-1635	66	2	.	.	X
eurjchem-1635	66	3	synthesis	synthesis	NOUN
eurjchem-1635	66	4	of	of	ADP
eurjchem-1635	66	5	4‐benzyl‐3,4‐dihydro‐2h‐benzo[b][1,4	4‐benzyl‐3,4‐dihydro‐2h‐benzo[b][1,4	PROPN
eurjchem-1635	66	6	]	]	PUNCT
eurjchem-1635	66	7	oxazine‐2‐carbonitrile	oxazine‐2‐carbonitrile	PROPN
eurjchem-1635	66	8	(	(	PUNCT
eurjchem-1635	66	9	2	2	NUM
eurjchem-1635	66	10	)	)	PUNCT
eurjchem-1635	66	11	to	to	ADP
eurjchem-1635	66	12	a	a	DET
eurjchem-1635	66	13	stirred	stir	VERB
eurjchem-1635	66	14	solution	solution	NOUN
eurjchem-1635	66	15	of	of	ADP
eurjchem-1635	66	16	compound	compound	NOUN
eurjchem-1635	66	17	1	1	NUM
eurjchem-1635	66	18	(	(	PUNCT
eurjchem-1635	66	19	1.6	1.6	NUM
eurjchem-1635	66	20	g	g	NOUN
eurjchem-1635	66	21	,	,	PUNCT
eurjchem-1635	66	22	10.0	10.0	NUM
eurjchem-1635	66	23	mmol	mmol	NOUN
eurjchem-1635	66	24	)	)	PUNCT
eurjchem-1635	66	25	in	in	ADP
eurjchem-1635	66	26	acetone	acetone	NOUN
eurjchem-1635	66	27	(	(	PUNCT
eurjchem-1635	66	28	32	32	NUM
eurjchem-1635	66	29	ml	ml	NOUN
eurjchem-1635	66	30	)	)	PUNCT
eurjchem-1635	66	31	was	be	AUX
eurjchem-1635	66	32	added	add	VERB
eurjchem-1635	66	33	2,6‐lutidine	2,6‐lutidine	NUM
eurjchem-1635	66	34	(	(	PUNCT
eurjchem-1635	66	35	2.14	2.14	NUM
eurjchem-1635	66	36	g	g	NOUN
eurjchem-1635	66	37	,	,	PUNCT
eurjchem-1635	66	38	20.0	20.0	NUM
eurjchem-1635	66	39	mmol	mmol	NOUN
eurjchem-1635	66	40	)	)	PUNCT
eurjchem-1635	66	41	386	386	NUM
eurjchem-1635	66	42	pawar	pawar	NOUN
eurjchem-1635	66	43	et	et	PROPN
eurjchem-1635	66	44	al	al	PROPN
eurjchem-1635	66	45	.	.	PUNCT
eurjchem-1635	66	46	/	/	SYM
eurjchem-1635	66	47	european	european	PROPN
eurjchem-1635	66	48	journal	journal	PROPN
eurjchem-1635	66	49	of	of	ADP
eurjchem-1635	66	50	chemistry	chemistry	NOUN
eurjchem-1635	66	51	8	8	NUM
eurjchem-1635	66	52	(	(	PUNCT
eurjchem-1635	66	53	4	4	NUM
eurjchem-1635	66	54	)	)	PUNCT
eurjchem-1635	66	55	(	(	PUNCT
eurjchem-1635	66	56	2017	2017	NUM
eurjchem-1635	66	57	)	)	PUNCT
eurjchem-1635	66	58	384‐390	384‐390	NUM
eurjchem-1635	66	59	and	and	CCONJ
eurjchem-1635	66	60	dimethyl	dimethyl	PROPN
eurjchem-1635	66	61	aminopyridine	aminopyridine	PROPN
eurjchem-1635	66	62	(	(	PUNCT
eurjchem-1635	66	63	dmap	dmap	NOUN
eurjchem-1635	66	64	)	)	PUNCT
eurjchem-1635	66	65	(	(	PUNCT
eurjchem-1635	66	66	0.24	0.24	NUM
eurjchem-1635	66	67	g	g	NOUN
eurjchem-1635	66	68	,	,	PUNCT
eurjchem-1635	66	69	2.00	2.00	NUM
eurjchem-1635	66	70	mmol	mmol	NOUN
eurjchem-1635	66	71	)	)	PUNCT
eurjchem-1635	66	72	the	the	DET
eurjchem-1635	66	73	mixture	mixture	NOUN
eurjchem-1635	66	74	was	be	AUX
eurjchem-1635	66	75	stirred	stir	VERB
eurjchem-1635	66	76	at	at	ADP
eurjchem-1635	66	77	room	room	NOUN
eurjchem-1635	66	78	temperature	temperature	NOUN
eurjchem-1635	66	79	for	for	ADP
eurjchem-1635	66	80	15	15	NUM
eurjchem-1635	66	81	min	min	NOUN
eurjchem-1635	66	82	,	,	PUNCT
eurjchem-1635	66	83	reaction	reaction	NOUN
eurjchem-1635	66	84	mixture	mixture	NOUN
eurjchem-1635	66	85	was	be	AUX
eurjchem-1635	66	86	cooled	cool	VERB
eurjchem-1635	66	87	to	to	ADP
eurjchem-1635	66	88	0	0	NUM
eurjchem-1635	66	89	°	°	NUM
eurjchem-1635	66	90	c	c	NOUN
eurjchem-1635	66	91	and	and	CCONJ
eurjchem-1635	66	92	1‐(bromomethyl)benzene	1‐(bromomethyl)benzene	NUM
eurjchem-1635	66	93	(	(	PUNCT
eurjchem-1635	66	94	2.05	2.05	NUM
eurjchem-1635	66	95	g	g	NOUN
eurjchem-1635	66	96	,	,	PUNCT
eurjchem-1635	66	97	12.0	12.0	NUM
eurjchem-1635	66	98	mmol	mmol	NOUN
eurjchem-1635	66	99	)	)	PUNCT
eurjchem-1635	66	100	was	be	AUX
eurjchem-1635	66	101	added	add	VERB
eurjchem-1635	66	102	drop	drop	NOUN
eurjchem-1635	66	103	wise	wise	ADJ
eurjchem-1635	66	104	followed	follow	VERB
eurjchem-1635	66	105	by	by	ADP
eurjchem-1635	66	106	stirring	stir	VERB
eurjchem-1635	66	107	at	at	ADP
eurjchem-1635	66	108	80	80	NUM
eurjchem-1635	66	109	°	°	NUM
eurjchem-1635	66	110	c	c	NOUN
eurjchem-1635	66	111	for	for	ADP
eurjchem-1635	66	112	1	1	NUM
eurjchem-1635	66	113	h.	h.	NOUN
eurjchem-1635	66	114	the	the	DET
eurjchem-1635	66	115	reaction	reaction	NOUN
eurjchem-1635	66	116	was	be	AUX
eurjchem-1635	66	117	monitored	monitor	VERB
eurjchem-1635	66	118	by	by	ADP
eurjchem-1635	66	119	tlc	tlc	NOUN
eurjchem-1635	66	120	and	and	CCONJ
eurjchem-1635	66	121	lc‐	lc‐	ADJ
eurjchem-1635	66	122	ms	ms	PROPN
eurjchem-1635	66	123	.	.	PROPN
eurjchem-1635	66	124	after	after	ADP
eurjchem-1635	66	125	completion	completion	NOUN
eurjchem-1635	66	126	the	the	DET
eurjchem-1635	66	127	reaction	reaction	NOUN
eurjchem-1635	66	128	,	,	PUNCT
eurjchem-1635	66	129	the	the	DET
eurjchem-1635	66	130	reaction	reaction	NOUN
eurjchem-1635	66	131	mass	mass	NOUN
eurjchem-1635	66	132	was	be	AUX
eurjchem-1635	66	133	evaporated	evaporate	VERB
eurjchem-1635	66	134	under	under	ADP
eurjchem-1635	66	135	reduced	reduce	VERB
eurjchem-1635	66	136	pressure	pressure	NOUN
eurjchem-1635	66	137	to	to	PART
eurjchem-1635	66	138	obtain	obtain	VERB
eurjchem-1635	66	139	crude	crude	ADJ
eurjchem-1635	66	140	gummy	gummy	ADJ
eurjchem-1635	66	141	material	material	NOUN
eurjchem-1635	66	142	.	.	PUNCT
eurjchem-1635	67	1	the	the	DET
eurjchem-1635	67	2	reaction	reaction	NOUN
eurjchem-1635	67	3	mixture	mixture	NOUN
eurjchem-1635	67	4	was	be	AUX
eurjchem-1635	67	5	diluted	dilute	VERB
eurjchem-1635	67	6	with	with	ADP
eurjchem-1635	67	7	h2o	h2o	PROPN
eurjchem-1635	67	8	(	(	PUNCT
eurjchem-1635	67	9	10	10	NUM
eurjchem-1635	67	10	ml	ml	NOUN
eurjchem-1635	67	11	)	)	PUNCT
eurjchem-1635	67	12	and	and	CCONJ
eurjchem-1635	67	13	extracted	extract	VERB
eurjchem-1635	67	14	with	with	ADP
eurjchem-1635	67	15	dichloromethane	dichloromethane	NOUN
eurjchem-1635	67	16	(	(	PUNCT
eurjchem-1635	67	17	dcm	dcm	PROPN
eurjchem-1635	67	18	)	)	PUNCT
eurjchem-1635	67	19	(	(	PUNCT
eurjchem-1635	67	20	2	2	NUM
eurjchem-1635	67	21	×	×	NOUN
eurjchem-1635	67	22	10	10	NUM
eurjchem-1635	67	23	ml	ml	NOUN
eurjchem-1635	67	24	)	)	PUNCT
eurjchem-1635	67	25	.	.	PUNCT
eurjchem-1635	68	1	the	the	DET
eurjchem-1635	68	2	organic	organic	ADJ
eurjchem-1635	68	3	layer	layer	NOUN
eurjchem-1635	68	4	was	be	AUX
eurjchem-1635	68	5	washed	wash	VERB
eurjchem-1635	68	6	with	with	ADP
eurjchem-1635	68	7	aq	aq	X
eurjchem-1635	68	8	.	.	NOUN
eurjchem-1635	68	9	saturated	saturate	VERB
eurjchem-1635	68	10	nahco3	nahco3	NOUN
eurjchem-1635	68	11	(	(	PUNCT
eurjchem-1635	68	12	15	15	NUM
eurjchem-1635	68	13	ml	ml	NOUN
eurjchem-1635	68	14	)	)	PUNCT
eurjchem-1635	68	15	,	,	PUNCT
eurjchem-1635	68	16	and	and	CCONJ
eurjchem-1635	68	17	brine	brine	NOUN
eurjchem-1635	68	18	(	(	PUNCT
eurjchem-1635	68	19	15	15	NUM
eurjchem-1635	68	20	ml	ml	NOUN
eurjchem-1635	68	21	)	)	PUNCT
eurjchem-1635	68	22	solution	solution	NOUN
eurjchem-1635	68	23	.	.	PUNCT
eurjchem-1635	69	1	separated	separate	VERB
eurjchem-1635	69	2	the	the	DET
eurjchem-1635	69	3	organic	organic	ADJ
eurjchem-1635	69	4	layer	layer	NOUN
eurjchem-1635	69	5	and	and	CCONJ
eurjchem-1635	69	6	dried	dry	VERB
eurjchem-1635	69	7	it	it	PRON
eurjchem-1635	69	8	over	over	ADP
eurjchem-1635	69	9	anhydrous	anhydrous	ADJ
eurjchem-1635	69	10	na2so4	na2so4	NOUN
eurjchem-1635	69	11	and	and	CCONJ
eurjchem-1635	69	12	evaporated	evaporate	VERB
eurjchem-1635	69	13	under	under	ADP
eurjchem-1635	69	14	reduced	reduce	VERB
eurjchem-1635	69	15	pressure	pressure	NOUN
eurjchem-1635	69	16	to	to	PART
eurjchem-1635	69	17	get	get	VERB
eurjchem-1635	69	18	4‐benzyl‐3,4‐dihydro‐2h‐benzo[b][1,4]oxazi	4‐benzyl‐3,4‐dihydro‐2h‐benzo[b][1,4]oxazi	NUM
eurjchem-1635	69	19	ne‐2‐carbonitrile	ne‐2‐carbonitrile	PROPN
eurjchem-1635	69	20	(	(	PUNCT
eurjchem-1635	69	21	2	2	NUM
eurjchem-1635	69	22	)	)	PUNCT
eurjchem-1635	69	23	.	.	PUNCT
eurjchem-1635	70	1	the	the	DET
eurjchem-1635	70	2	product	product	NOUN
eurjchem-1635	70	3	was	be	AUX
eurjchem-1635	70	4	confirmed	confirm	VERB
eurjchem-1635	70	5	by	by	ADP
eurjchem-1635	70	6	nmr	nmr	NOUN
eurjchem-1635	70	7	and	and	CCONJ
eurjchem-1635	70	8	lc‐ms	lc‐ms	NOUN
eurjchem-1635	70	9	and	and	CCONJ
eurjchem-1635	70	10	used	use	VERB
eurjchem-1635	70	11	as	as	ADP
eurjchem-1635	70	12	such	such	ADJ
eurjchem-1635	70	13	for	for	ADP
eurjchem-1635	70	14	next	next	ADJ
eurjchem-1635	70	15	step	step	NOUN
eurjchem-1635	70	16	(	(	PUNCT
eurjchem-1635	70	17	scheme	scheme	NOUN
eurjchem-1635	70	18	1	1	NUM
eurjchem-1635	70	19	)	)	PUNCT
eurjchem-1635	70	20	.	.	PUNCT
eurjchem-1635	71	1	color	color	NOUN
eurjchem-1635	71	2	:	:	PUNCT
eurjchem-1635	71	3	yellow	yellow	ADJ
eurjchem-1635	71	4	.	.	PUNCT
eurjchem-1635	72	1	yield	yield	NOUN
eurjchem-1635	72	2	:	:	PUNCT
eurjchem-1635	72	3	2.25	2.25	NUM
eurjchem-1635	72	4	g	g	NOUN
eurjchem-1635	72	5	,	,	PUNCT
eurjchem-1635	72	6	90	90	NUM
eurjchem-1635	72	7	%	%	NOUN
eurjchem-1635	72	8	.	.	PUNCT
eurjchem-1635	73	1	ms	ms	NOUN
eurjchem-1635	73	2	(	(	PUNCT
eurjchem-1635	73	3	esi	esi	PROPN
eurjchem-1635	73	4	,	,	PUNCT
eurjchem-1635	73	5	m	m	PROPN
eurjchem-1635	73	6	/	/	SYM
eurjchem-1635	73	7	z	z	NOUN
eurjchem-1635	73	8	):	):	PUNCT
eurjchem-1635	73	9	251	251	NUM
eurjchem-1635	74	1	[	[	X
eurjchem-1635	74	2	m+h]+	m+h]+	X
eurjchem-1635	74	3	.	.	PUNCT
eurjchem-1635	74	4	1h	1h	NUM
eurjchem-1635	74	5	nmr	nmr	NOUN
eurjchem-1635	74	6	(	(	PUNCT
eurjchem-1635	74	7	400	400	NUM
eurjchem-1635	74	8	mhz	mhz	NOUN
eurjchem-1635	74	9	,	,	PUNCT
eurjchem-1635	74	10	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	74	11	,	,	PUNCT
eurjchem-1635	74	12	δ	δ	PROPN
eurjchem-1635	74	13	,	,	PUNCT
eurjchem-1635	74	14	ppm	ppm	NUM
eurjchem-1635	74	15	):	):	PUNCT
eurjchem-1635	74	16	7.42‐7.18	7.42‐7.18	NUM
eurjchem-1635	74	17	(	(	PUNCT
eurjchem-1635	74	18	m	m	PROPN
eurjchem-1635	74	19	,	,	PUNCT
eurjchem-1635	74	20	5h	5h	NUM
eurjchem-1635	74	21	,	,	PUNCT
eurjchem-1635	74	22	ar‐h	ar‐h	NOUN
eurjchem-1635	74	23	)	)	PUNCT
eurjchem-1635	74	24	,	,	PUNCT
eurjchem-1635	74	25	6.83‐	6.83‐	NUM
eurjchem-1635	74	26	6.79	6.79	NUM
eurjchem-1635	74	27	(	(	PUNCT
eurjchem-1635	74	28	m	m	PROPN
eurjchem-1635	74	29	,	,	PUNCT
eurjchem-1635	74	30	2h	2h	NUM
eurjchem-1635	74	31	,	,	PUNCT
eurjchem-1635	74	32	ar‐h	ar‐h	NOUN
eurjchem-1635	74	33	)	)	PUNCT
eurjchem-1635	74	34	,	,	PUNCT
eurjchem-1635	74	35	6.63‐6.58	6.63‐6.58	NUM
eurjchem-1635	74	36	(	(	PUNCT
eurjchem-1635	74	37	m	m	PROPN
eurjchem-1635	74	38	,	,	PUNCT
eurjchem-1635	74	39	2h	2h	NUM
eurjchem-1635	74	40	,	,	PUNCT
eurjchem-1635	74	41	ar‐h	ar‐h	NOUN
eurjchem-1635	74	42	)	)	PUNCT
eurjchem-1635	74	43	,	,	PUNCT
eurjchem-1635	74	44	5.68	5.68	NUM
eurjchem-1635	74	45	(	(	PUNCT
eurjchem-1635	74	46	m	m	PROPN
eurjchem-1635	74	47	,	,	PUNCT
eurjchem-1635	74	48	1h	1h	NUM
eurjchem-1635	74	49	,	,	PUNCT
eurjchem-1635	74	50	cn‐	cn‐	PROPN
eurjchem-1635	74	51	ch	ch	NOUN
eurjchem-1635	74	52	)	)	PUNCT
eurjchem-1635	74	53	,	,	PUNCT
eurjchem-1635	74	54	4.42‐4.39	4.42‐4.39	NUM
eurjchem-1635	74	55	(	(	PUNCT
eurjchem-1635	74	56	q	q	NOUN
eurjchem-1635	74	57	,	,	PUNCT
eurjchem-1635	74	58	2h	2h	NUM
eurjchem-1635	74	59	,	,	PUNCT
eurjchem-1635	74	60	ph‐ch2	ph‐ch2	ADJ
eurjchem-1635	74	61	)	)	PUNCT
eurjchem-1635	74	62	,	,	PUNCT
eurjchem-1635	74	63	3.63‐3.57	3.63‐3.57	NUM
eurjchem-1635	74	64	(	(	PUNCT
eurjchem-1635	74	65	q	q	NOUN
eurjchem-1635	74	66	,	,	PUNCT
eurjchem-1635	74	67	2h	2h	NUM
eurjchem-1635	74	68	,	,	PUNCT
eurjchem-1635	74	69	n‐ch2	n‐ch2	PROPN
eurjchem-1635	74	70	)	)	PUNCT
eurjchem-1635	74	71	.	.	PUNCT
eurjchem-1635	75	1	2.2.3	2.2.3	X
eurjchem-1635	75	2	.	.	X
eurjchem-1635	75	3	synthesis	synthesis	NOUN
eurjchem-1635	75	4	of	of	ADP
eurjchem-1635	75	5	(	(	PUNCT
eurjchem-1635	75	6	4‐benzyl‐3,4‐dihydro‐2h‐benzo[b][1,4	4‐benzyl‐3,4‐dihydro‐2h‐benzo[b][1,4	PROPN
eurjchem-1635	75	7	]	]	X
eurjchem-1635	75	8	oxazin‐2‐yl)methanamine	oxazin‐2‐yl)methanamine	PROPN
eurjchem-1635	75	9	(	(	PUNCT
eurjchem-1635	75	10	3	3	NUM
eurjchem-1635	75	11	)	)	PUNCT
eurjchem-1635	75	12	to	to	ADP
eurjchem-1635	75	13	a	a	DET
eurjchem-1635	75	14	stirred	stir	VERB
eurjchem-1635	75	15	solution	solution	NOUN
eurjchem-1635	75	16	of	of	ADP
eurjchem-1635	75	17	compound	compound	NOUN
eurjchem-1635	75	18	2	2	NUM
eurjchem-1635	75	19	(	(	PUNCT
eurjchem-1635	75	20	0.25	0.25	NUM
eurjchem-1635	75	21	g	g	NOUN
eurjchem-1635	75	22	,	,	PUNCT
eurjchem-1635	75	23	1.00	1.00	NUM
eurjchem-1635	75	24	mmol	mmol	NOUN
eurjchem-1635	75	25	)	)	PUNCT
eurjchem-1635	75	26	in	in	ADP
eurjchem-1635	75	27	parr	parr	PROPN
eurjchem-1635	75	28	shaker	shaker	NOUN
eurjchem-1635	75	29	vessel	vessel	NOUN
eurjchem-1635	75	30	added	add	VERB
eurjchem-1635	75	31	methanolic	methanolic	NOUN
eurjchem-1635	75	32	ammonia	ammonia	NOUN
eurjchem-1635	75	33	(	(	PUNCT
eurjchem-1635	75	34	2.5	2.5	NUM
eurjchem-1635	75	35	ml	ml	NOUN
eurjchem-1635	75	36	)	)	PUNCT
eurjchem-1635	75	37	and	and	CCONJ
eurjchem-1635	75	38	then	then	ADV
eurjchem-1635	75	39	added	add	VERB
eurjchem-1635	75	40	raney	raney	PROPN
eurjchem-1635	75	41	ni	ni	PROPN
eurjchem-1635	75	42	(	(	PUNCT
eurjchem-1635	75	43	0.05	0.05	NUM
eurjchem-1635	75	44	g	g	NOUN
eurjchem-1635	75	45	)	)	PUNCT
eurjchem-1635	75	46	and	and	CCONJ
eurjchem-1635	75	47	kept	keep	VERB
eurjchem-1635	75	48	reaction	reaction	NOUN
eurjchem-1635	75	49	mixture	mixture	NOUN
eurjchem-1635	75	50	hydrogen	hydrogen	NOUN
eurjchem-1635	75	51	gas	gas	NOUN
eurjchem-1635	75	52	pressure	pressure	NOUN
eurjchem-1635	75	53	of	of	ADP
eurjchem-1635	75	54	60	60	NUM
eurjchem-1635	75	55	psi	psi	NOUN
eurjchem-1635	75	56	for	for	ADP
eurjchem-1635	75	57	3	3	NUM
eurjchem-1635	75	58	h.	h.	NOUN
eurjchem-1635	75	59	progress	progress	NOUN
eurjchem-1635	75	60	of	of	ADP
eurjchem-1635	75	61	reaction	reaction	NOUN
eurjchem-1635	75	62	was	be	AUX
eurjchem-1635	75	63	monitored	monitor	VERB
eurjchem-1635	75	64	by	by	ADP
eurjchem-1635	75	65	tlc	tlc	PROPN
eurjchem-1635	75	66	.	.	PUNCT
eurjchem-1635	76	1	filtered	filter	VERB
eurjchem-1635	76	2	reaction	reaction	NOUN
eurjchem-1635	76	3	mass	mass	NOUN
eurjchem-1635	76	4	through	through	ADP
eurjchem-1635	76	5	a	a	DET
eurjchem-1635	76	6	pad	pad	NOUN
eurjchem-1635	76	7	of	of	ADP
eurjchem-1635	76	8	celite	celite	ADJ
eurjchem-1635	76	9	and	and	CCONJ
eurjchem-1635	76	10	obtain	obtain	VERB
eurjchem-1635	76	11	filtrate	filtrate	NOUN
eurjchem-1635	76	12	.	.	PUNCT
eurjchem-1635	77	1	evaporated	evaporate	VERB
eurjchem-1635	77	2	it	it	PRON
eurjchem-1635	77	3	under	under	ADP
eurjchem-1635	77	4	reduced	reduced	ADJ
eurjchem-1635	77	5	pres‐	pres‐	NOUN
eurjchem-1635	77	6	sure	sure	ADJ
eurjchem-1635	77	7	to	to	PART
eurjchem-1635	77	8	obtain	obtain	VERB
eurjchem-1635	77	9	crude	crude	ADJ
eurjchem-1635	77	10	yellow	yellow	ADJ
eurjchem-1635	77	11	gummy	gummy	ADJ
eurjchem-1635	77	12	mass	mass	NOUN
eurjchem-1635	77	13	which	which	PRON
eurjchem-1635	77	14	was	be	AUX
eurjchem-1635	77	15	washed	wash	VERB
eurjchem-1635	77	16	by	by	ADP
eurjchem-1635	77	17	etoac	etoac	ADJ
eurjchem-1635	77	18	:	:	PUNCT
eurjchem-1635	77	19	hexane	hexane	ADJ
eurjchem-1635	77	20	mixture	mixture	NOUN
eurjchem-1635	77	21	(	(	PUNCT
eurjchem-1635	77	22	10:90	10:90	NUM
eurjchem-1635	77	23	,	,	PUNCT
eurjchem-1635	77	24	v	v	NOUN
eurjchem-1635	77	25	:	:	PUNCT
eurjchem-1635	77	26	v	v	NOUN
eurjchem-1635	77	27	,	,	PUNCT
eurjchem-1635	77	28	5	5	NUM
eurjchem-1635	77	29	ml	ml	NOUN
eurjchem-1635	77	30	)	)	PUNCT
eurjchem-1635	77	31	,	,	PUNCT
eurjchem-1635	77	32	the	the	DET
eurjchem-1635	77	33	gummy	gummy	ADJ
eurjchem-1635	77	34	mass	mass	NOUN
eurjchem-1635	77	35	later	later	ADV
eurjchem-1635	77	36	solidified	solidify	VERB
eurjchem-1635	77	37	on	on	ADP
eurjchem-1635	77	38	standing	stand	VERB
eurjchem-1635	77	39	and	and	CCONJ
eurjchem-1635	77	40	obtain	obtain	VERB
eurjchem-1635	77	41	(	(	PUNCT
eurjchem-1635	77	42	4‐benzyl‐3,4‐dihydro‐	4‐benzyl‐3,4‐dihydro‐	NUM
eurjchem-1635	77	43	2h‐benzo[b][1,4]oxazin‐2‐yl)methanamine	2h‐benzo[b][1,4]oxazin‐2‐yl)methanamine	NOUN
eurjchem-1635	77	44	(	(	PUNCT
eurjchem-1635	77	45	3	3	NUM
eurjchem-1635	77	46	)	)	PUNCT
eurjchem-1635	77	47	as	as	ADP
eurjchem-1635	77	48	a	a	DET
eurjchem-1635	77	49	yellow	yellow	ADJ
eurjchem-1635	77	50	solid	solid	ADJ
eurjchem-1635	77	51	(	(	PUNCT
eurjchem-1635	77	52	scheme	scheme	NOUN
eurjchem-1635	77	53	1	1	NUM
eurjchem-1635	77	54	)	)	PUNCT
eurjchem-1635	77	55	.	.	PUNCT
eurjchem-1635	78	1	color	color	NOUN
eurjchem-1635	78	2	:	:	PUNCT
eurjchem-1635	78	3	yellow	yellow	ADJ
eurjchem-1635	78	4	.	.	PUNCT
eurjchem-1635	79	1	yield	yield	NOUN
eurjchem-1635	79	2	:	:	PUNCT
eurjchem-1635	79	3	0.22	0.22	NUM
eurjchem-1635	79	4	g	g	NOUN
eurjchem-1635	79	5	,	,	PUNCT
eurjchem-1635	79	6	85	85	NUM
eurjchem-1635	79	7	%	%	NOUN
eurjchem-1635	79	8	.	.	PUNCT
eurjchem-1635	80	1	ms	ms	NOUN
eurjchem-1635	80	2	(	(	PUNCT
eurjchem-1635	80	3	esi	esi	PROPN
eurjchem-1635	80	4	,	,	PUNCT
eurjchem-1635	80	5	m	m	PROPN
eurjchem-1635	80	6	/	/	SYM
eurjchem-1635	80	7	z	z	NOUN
eurjchem-1635	80	8	):	):	PUNCT
eurjchem-1635	80	9	255	255	NUM
eurjchem-1635	81	1	[	[	X
eurjchem-1635	81	2	m+h]+	m+h]+	X
eurjchem-1635	81	3	.	.	PUNCT
eurjchem-1635	82	1	1h	1h	NUM
eurjchem-1635	82	2	nmr	nmr	NOUN
eurjchem-1635	82	3	(	(	PUNCT
eurjchem-1635	82	4	400	400	NUM
eurjchem-1635	82	5	mhz	mhz	NOUN
eurjchem-1635	82	6	,	,	PUNCT
eurjchem-1635	82	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	82	8	,	,	PUNCT
eurjchem-1635	82	9	δ	δ	PROPN
eurjchem-1635	82	10	,	,	PUNCT
eurjchem-1635	82	11	ppm	ppm	NOUN
eurjchem-1635	82	12	):	):	PUNCT
eurjchem-1635	82	13	7.38‐	7.38‐	NUM
eurjchem-1635	82	14	7.28	7.28	NUM
eurjchem-1635	82	15	(	(	PUNCT
eurjchem-1635	82	16	m	m	PROPN
eurjchem-1635	82	17	,	,	PUNCT
eurjchem-1635	82	18	5h	5h	NUM
eurjchem-1635	82	19	,	,	PUNCT
eurjchem-1635	82	20	ar‐h	ar‐h	NOUN
eurjchem-1635	82	21	)	)	PUNCT
eurjchem-1635	82	22	,	,	PUNCT
eurjchem-1635	82	23	6.8‐6.73	6.8‐6.73	NUM
eurjchem-1635	82	24	(	(	PUNCT
eurjchem-1635	82	25	m	m	PROPN
eurjchem-1635	82	26	,	,	PUNCT
eurjchem-1635	82	27	2h	2h	NUM
eurjchem-1635	82	28	,	,	PUNCT
eurjchem-1635	82	29	ar‐h	ar‐h	NOUN
eurjchem-1635	82	30	)	)	PUNCT
eurjchem-1635	82	31	,	,	PUNCT
eurjchem-1635	82	32	6.64‐6.51	6.64‐6.51	PROPN
eurjchem-1635	82	33	(	(	PUNCT
eurjchem-1635	82	34	m	m	PROPN
eurjchem-1635	82	35	,	,	PUNCT
eurjchem-1635	82	36	2h	2h	NUM
eurjchem-1635	82	37	,	,	PUNCT
eurjchem-1635	82	38	ar‐h	ar‐h	NOUN
eurjchem-1635	82	39	)	)	PUNCT
eurjchem-1635	82	40	,	,	PUNCT
eurjchem-1635	82	41	5.48	5.48	NUM
eurjchem-1635	82	42	(	(	PUNCT
eurjchem-1635	82	43	m	m	PROPN
eurjchem-1635	82	44	,	,	PUNCT
eurjchem-1635	82	45	1h	1h	NUM
eurjchem-1635	82	46	,	,	PUNCT
eurjchem-1635	82	47	ch2‐ch	ch2‐ch	NOUN
eurjchem-1635	82	48	)	)	PUNCT
eurjchem-1635	82	49	,	,	PUNCT
eurjchem-1635	82	50	4.12‐4.10	4.12‐4.10	NUM
eurjchem-1635	82	51	(	(	PUNCT
eurjchem-1635	82	52	m	m	PROPN
eurjchem-1635	82	53	,	,	PUNCT
eurjchem-1635	82	54	2h	2h	NUM
eurjchem-1635	82	55	,	,	PUNCT
eurjchem-1635	82	56	ph‐ch2	ph‐ch2	ADJ
eurjchem-1635	82	57	)	)	PUNCT
eurjchem-1635	82	58	,	,	PUNCT
eurjchem-1635	82	59	3.63‐	3.63‐	NUM
eurjchem-1635	82	60	3.57	3.57	NUM
eurjchem-1635	82	61	(	(	PUNCT
eurjchem-1635	82	62	m	m	PROPN
eurjchem-1635	82	63	,	,	PUNCT
eurjchem-1635	82	64	2h	2h	NUM
eurjchem-1635	82	65	,	,	PUNCT
eurjchem-1635	82	66	n‐ch2	n‐ch2	PROPN
eurjchem-1635	82	67	)	)	PUNCT
eurjchem-1635	82	68	,	,	PUNCT
eurjchem-1635	82	69	3.15‐3.07	3.15‐3.07	NUM
eurjchem-1635	82	70	(	(	PUNCT
eurjchem-1635	82	71	m	m	PROPN
eurjchem-1635	82	72	,	,	PUNCT
eurjchem-1635	82	73	2h	2h	NUM
eurjchem-1635	82	74	,	,	PUNCT
eurjchem-1635	82	75	nh2‐ch2	nh2‐ch2	PROPN
eurjchem-1635	82	76	)	)	PUNCT
eurjchem-1635	82	77	,	,	PUNCT
eurjchem-1635	82	78	2.10	2.10	NUM
eurjchem-1635	82	79	(	(	PUNCT
eurjchem-1635	82	80	br	br	NOUN
eurjchem-1635	82	81	,	,	PUNCT
eurjchem-1635	82	82	2h	2h	NUM
eurjchem-1635	82	83	,	,	PUNCT
eurjchem-1635	82	84	ch2‐nh2	ch2‐nh2	PROPN
eurjchem-1635	82	85	)	)	PUNCT
eurjchem-1635	82	86	.	.	PUNCT
eurjchem-1635	83	1	2.2.4	2.2.4	NUM
eurjchem-1635	83	2	.	.	PUNCT
eurjchem-1635	83	3	general	general	ADJ
eurjchem-1635	83	4	procedure	procedure	NOUN
eurjchem-1635	83	5	for	for	ADP
eurjchem-1635	83	6	the	the	DET
eurjchem-1635	83	7	synthesis	synthesis	NOUN
eurjchem-1635	83	8	of	of	ADP
eurjchem-1635	83	9	n‐((4‐benzyl‐	n‐((4‐benzyl‐	PROPN
eurjchem-1635	83	10	3,4‐dihydro‐2h‐benzo[b][1,4]oxazin‐2‐yl)methyl)‐4‐	3,4‐dihydro‐2h‐benzo[b][1,4]oxazin‐2‐yl)methyl)‐4‐	NUM
eurjchem-1635	83	11	substituted‐sulfonamide	substituted‐sulfonamide	ADV
eurjchem-1635	83	12	derivatives	derivative	NOUN
eurjchem-1635	83	13	(	(	PUNCT
eurjchem-1635	83	14	4a‐4e	4a‐4e	NOUN
eurjchem-1635	83	15	)	)	PUNCT
eurjchem-1635	83	16	to	to	ADP
eurjchem-1635	83	17	a	a	DET
eurjchem-1635	83	18	stirred	stir	VERB
eurjchem-1635	83	19	solution	solution	NOUN
eurjchem-1635	83	20	compound	compound	NOUN
eurjchem-1635	83	21	3	3	NUM
eurjchem-1635	83	22	(	(	PUNCT
eurjchem-1635	83	23	1	1	NUM
eurjchem-1635	83	24	equiv	equiv	NOUN
eurjchem-1635	83	25	.	.	PUNCT
eurjchem-1635	83	26	)	)	PUNCT
eurjchem-1635	84	1	in	in	ADP
eurjchem-1635	84	2	dcm	dcm	PROPN
eurjchem-1635	84	3	(	(	PUNCT
eurjchem-1635	84	4	10	10	NUM
eurjchem-1635	84	5	times	time	NOUN
eurjchem-1635	84	6	)	)	PUNCT
eurjchem-1635	84	7	was	be	AUX
eurjchem-1635	84	8	added	add	VERB
eurjchem-1635	84	9	pyridine	pyridine	NOUN
eurjchem-1635	84	10	(	(	PUNCT
eurjchem-1635	84	11	10	10	NUM
eurjchem-1635	84	12	times	time	NOUN
eurjchem-1635	84	13	)	)	PUNCT
eurjchem-1635	84	14	the	the	DET
eurjchem-1635	84	15	mixture	mixture	NOUN
eurjchem-1635	84	16	was	be	AUX
eurjchem-1635	84	17	stirred	stir	VERB
eurjchem-1635	84	18	at	at	ADP
eurjchem-1635	84	19	room	room	NOUN
eurjchem-1635	84	20	temperature	temperature	NOUN
eurjchem-1635	84	21	for	for	ADP
eurjchem-1635	84	22	15	15	NUM
eurjchem-1635	84	23	min	min	NOUN
eurjchem-1635	84	24	.	.	PROPN
eurjchem-1635	84	25	reaction	reaction	NOUN
eurjchem-1635	84	26	mixture	mixture	NOUN
eurjchem-1635	84	27	was	be	AUX
eurjchem-1635	84	28	cooled	cool	VERB
eurjchem-1635	84	29	to	to	ADP
eurjchem-1635	84	30	0	0	NUM
eurjchem-1635	84	31	°	°	ADP
eurjchem-1635	84	32	c	c	NOUN
eurjchem-1635	84	33	and	and	CCONJ
eurjchem-1635	84	34	substituted	substitute	VERB
eurjchem-1635	84	35	sulfonyl	sulfonyl	NOUN
eurjchem-1635	84	36	chloride	chloride	NOUN
eurjchem-1635	84	37	(	(	PUNCT
eurjchem-1635	84	38	1.2	1.2	NUM
eurjchem-1635	84	39	equiv	equiv	NOUN
eurjchem-1635	84	40	.	.	PUNCT
eurjchem-1635	84	41	)	)	PUNCT
eurjchem-1635	84	42	was	be	AUX
eurjchem-1635	84	43	added	add	VERB
eurjchem-1635	84	44	drop	drop	NOUN
eurjchem-1635	84	45	wise	wise	ADJ
eurjchem-1635	84	46	followed	follow	VERB
eurjchem-1635	84	47	by	by	ADP
eurjchem-1635	84	48	stirring	stir	VERB
eurjchem-1635	84	49	at	at	ADP
eurjchem-1635	84	50	room	room	NOUN
eurjchem-1635	84	51	temperature	temperature	NOUN
eurjchem-1635	84	52	for	for	ADP
eurjchem-1635	84	53	6	6	NUM
eurjchem-1635	84	54	h.	h.	NOUN
eurjchem-1635	84	55	the	the	DET
eurjchem-1635	84	56	reaction	reaction	NOUN
eurjchem-1635	84	57	was	be	AUX
eurjchem-1635	84	58	monitored	monitor	VERB
eurjchem-1635	84	59	by	by	ADP
eurjchem-1635	84	60	tlc	tlc	NOUN
eurjchem-1635	84	61	and	and	CCONJ
eurjchem-1635	84	62	lc‐ms	lc‐ms	NUM
eurjchem-1635	84	63	,	,	PUNCT
eurjchem-1635	84	64	after	after	ADP
eurjchem-1635	84	65	completion	completion	NOUN
eurjchem-1635	84	66	of	of	ADP
eurjchem-1635	84	67	reaction	reaction	NOUN
eurjchem-1635	84	68	,	,	PUNCT
eurjchem-1635	84	69	the	the	DET
eurjchem-1635	84	70	reaction	reaction	NOUN
eurjchem-1635	84	71	mass	mass	NOUN
eurjchem-1635	84	72	was	be	AUX
eurjchem-1635	84	73	diluted	dilute	VERB
eurjchem-1635	84	74	with	with	ADP
eurjchem-1635	84	75	cold	cold	ADJ
eurjchem-1635	84	76	2	2	NUM
eurjchem-1635	84	77	n	n	NOUN
eurjchem-1635	84	78	hcl	hcl	NOUN
eurjchem-1635	84	79	and	and	CCONJ
eurjchem-1635	84	80	stirred	stir	VERB
eurjchem-1635	84	81	it	it	PRON
eurjchem-1635	84	82	for	for	ADP
eurjchem-1635	84	83	30	30	NUM
eurjchem-1635	84	84	min	min	NOUN
eurjchem-1635	84	85	.	.	PUNCT
eurjchem-1635	85	1	the	the	DET
eurjchem-1635	85	2	precipitation	precipitation	NOUN
eurjchem-1635	85	3	formed	form	VERB
eurjchem-1635	85	4	in	in	ADP
eurjchem-1635	85	5	reaction	reaction	NOUN
eurjchem-1635	85	6	mixture	mixture	NOUN
eurjchem-1635	85	7	.	.	PUNCT
eurjchem-1635	86	1	filtered	filter	VERB
eurjchem-1635	86	2	the	the	DET
eurjchem-1635	86	3	obtained	obtain	VERB
eurjchem-1635	86	4	solid	solid	ADJ
eurjchem-1635	86	5	and	and	CCONJ
eurjchem-1635	86	6	washed	wash	VERB
eurjchem-1635	86	7	it	it	PRON
eurjchem-1635	86	8	with	with	ADP
eurjchem-1635	86	9	excess	excess	NOUN
eurjchem-1635	86	10	of	of	ADP
eurjchem-1635	86	11	water	water	NOUN
eurjchem-1635	86	12	and	and	CCONJ
eurjchem-1635	86	13	cold	cold	ADJ
eurjchem-1635	86	14	diethyl	diethyl	NOUN
eurjchem-1635	86	15	ether	ether	NOUN
eurjchem-1635	86	16	and	and	CCONJ
eurjchem-1635	86	17	cold	cold	ADJ
eurjchem-1635	86	18	pentane	pentane	NOUN
eurjchem-1635	86	19	to	to	PART
eurjchem-1635	86	20	obtain	obtain	VERB
eurjchem-1635	86	21	all	all	DET
eurjchem-1635	86	22	compounds	compound	NOUN
eurjchem-1635	86	23	as	as	ADP
eurjchem-1635	86	24	white	white	ADJ
eurjchem-1635	86	25	solids	solid	NOUN
eurjchem-1635	86	26	.	.	PUNCT
eurjchem-1635	87	1	for	for	ADP
eurjchem-1635	87	2	filtrate	filtrate	NOUN
eurjchem-1635	87	3	extracted	extract	VERB
eurjchem-1635	87	4	with	with	ADP
eurjchem-1635	87	5	dcm	dcm	PROPN
eurjchem-1635	87	6	twice	twice	ADV
eurjchem-1635	87	7	.	.	PUNCT
eurjchem-1635	88	1	the	the	DET
eurjchem-1635	88	2	organic	organic	ADJ
eurjchem-1635	88	3	layer	layer	NOUN
eurjchem-1635	88	4	was	be	AUX
eurjchem-1635	88	5	washed	wash	VERB
eurjchem-1635	88	6	with	with	ADP
eurjchem-1635	88	7	brine	brine	NOUN
eurjchem-1635	88	8	solution	solution	NOUN
eurjchem-1635	88	9	;	;	PUNCT
eurjchem-1635	88	10	organic	organic	ADJ
eurjchem-1635	88	11	layer	layer	NOUN
eurjchem-1635	88	12	was	be	AUX
eurjchem-1635	88	13	evaporated	evaporate	VERB
eurjchem-1635	88	14	under	under	ADP
eurjchem-1635	88	15	reduced	reduce	VERB
eurjchem-1635	88	16	pressure	pressure	NOUN
eurjchem-1635	88	17	to	to	PART
eurjchem-1635	88	18	get	get	AUX
eurjchem-1635	88	19	desired	desire	VERB
eurjchem-1635	88	20	4‐substituted‐3,4‐dihydro‐2h‐benzo	4‐substituted‐3,4‐dihydro‐2h‐benzo	NUM
eurjchem-1635	88	21	[	[	X
eurjchem-1635	88	22	b][1,4]oxazin‐2‐yl)methane	b][1,4]oxazin‐2‐yl)methane	NOUN
eurjchem-1635	88	23	substituted	substitute	VERB
eurjchem-1635	88	24	sulfonamide	sulfonamide	NOUN
eurjchem-1635	88	25	(	(	PUNCT
eurjchem-1635	88	26	4a‐e	4a‐e	NOUN
eurjchem-1635	88	27	)	)	PUNCT
eurjchem-1635	88	28	derivatives	derivative	NOUN
eurjchem-1635	88	29	as	as	ADP
eurjchem-1635	88	30	white	white	ADJ
eurjchem-1635	88	31	solids	solid	NOUN
eurjchem-1635	88	32	(	(	PUNCT
eurjchem-1635	88	33	scheme	scheme	NOUN
eurjchem-1635	88	34	1	1	NUM
eurjchem-1635	88	35	)	)	PUNCT
eurjchem-1635	88	36	.	.	PUNCT
eurjchem-1635	89	1	n‐((4‐benzyl‐3	n‐((4‐benzyl‐3	NOUN
eurjchem-1635	89	2	,	,	PUNCT
eurjchem-1635	89	3	4‐dihydro‐2h‐benzo[b][1	4‐dihydro‐2h‐benzo[b][1	NOUN
eurjchem-1635	89	4	,	,	PUNCT
eurjchem-1635	89	5	4]oxazin‐2‐yl	4]oxazin‐2‐yl	NUM
eurjchem-1635	89	6	)	)	PUNCT
eurjchem-1635	90	1	methyl)benzenesulfonamide	methyl)benzenesulfonamide	ADP
eurjchem-1635	90	2	(	(	PUNCT
eurjchem-1635	90	3	4a	4a	NUM
eurjchem-1635	90	4	):	):	PUNCT
eurjchem-1635	90	5	color	color	NOUN
eurjchem-1635	90	6	:	:	PUNCT
eurjchem-1635	90	7	white	white	ADJ
eurjchem-1635	90	8	.	.	PUNCT
eurjchem-1635	91	1	yield	yield	NOUN
eurjchem-1635	91	2	:	:	PUNCT
eurjchem-1635	91	3	92	92	NUM
eurjchem-1635	91	4	%	%	NOUN
eurjchem-1635	91	5	.	.	PUNCT
eurjchem-1635	92	1	m.p	m.p	PROPN
eurjchem-1635	92	2	.	.	PROPN
eurjchem-1635	92	3	:	:	PUNCT
eurjchem-1635	93	1	175‐176	175‐176	PROPN
eurjchem-1635	93	2	°	°	PROPN
eurjchem-1635	93	3	c	c	PROPN
eurjchem-1635	93	4	.	.	PUNCT
eurjchem-1635	94	1	1h	1h	NUM
eurjchem-1635	94	2	nmr	nmr	NOUN
eurjchem-1635	94	3	(	(	PUNCT
eurjchem-1635	94	4	400	400	NUM
eurjchem-1635	94	5	mhz	mhz	NOUN
eurjchem-1635	94	6	,	,	PUNCT
eurjchem-1635	94	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	94	8	,	,	PUNCT
eurjchem-1635	94	9	δ	δ	PROPN
eurjchem-1635	94	10	,	,	PUNCT
eurjchem-1635	94	11	ppm	ppm	NUM
eurjchem-1635	94	12	):	):	PUNCT
eurjchem-1635	94	13	7.98	7.98	NUM
eurjchem-1635	94	14	(	(	PUNCT
eurjchem-1635	94	15	t	t	PROPN
eurjchem-1635	94	16	,	,	PUNCT
eurjchem-1635	94	17	1h	1h	NUM
eurjchem-1635	94	18	,	,	PUNCT
eurjchem-1635	94	19	j	j	PROPN
eurjchem-1635	94	20	=	=	SYM
eurjchem-1635	94	21	6	6	NUM
eurjchem-1635	94	22	hz	hz	NOUN
eurjchem-1635	94	23	,	,	PUNCT
eurjchem-1635	94	24	nh	nh	PROPN
eurjchem-1635	94	25	)	)	PUNCT
eurjchem-1635	94	26	,	,	PUNCT
eurjchem-1635	94	27	7.82‐7.80	7.82‐7.80	NUM
eurjchem-1635	94	28	(	(	PUNCT
eurjchem-1635	94	29	d	d	NOUN
eurjchem-1635	94	30	,	,	PUNCT
eurjchem-1635	94	31	2h	2h	NUM
eurjchem-1635	94	32	,	,	PUNCT
eurjchem-1635	94	33	j	j	PROPN
eurjchem-1635	94	34	=	=	SYM
eurjchem-1635	94	35	6.8	6.8	NUM
eurjchem-1635	94	36	hz	hz	NOUN
eurjchem-1635	94	37	,	,	PUNCT
eurjchem-1635	94	38	ar‐h	ar‐h	NOUN
eurjchem-1635	94	39	)	)	PUNCT
eurjchem-1635	94	40	,	,	PUNCT
eurjchem-1635	94	41	7.66‐7.57	7.66‐7.57	NUM
eurjchem-1635	94	42	(	(	PUNCT
eurjchem-1635	94	43	m	m	PROPN
eurjchem-1635	94	44	,	,	PUNCT
eurjchem-1635	94	45	3h	3h	NUM
eurjchem-1635	94	46	,	,	PUNCT
eurjchem-1635	94	47	ar‐h	ar‐h	NOUN
eurjchem-1635	94	48	)	)	PUNCT
eurjchem-1635	94	49	,	,	PUNCT
eurjchem-1635	94	50	7.34‐7.24	7.34‐7.24	NUM
eurjchem-1635	94	51	(	(	PUNCT
eurjchem-1635	94	52	dd	dd	NOUN
eurjchem-1635	94	53	,	,	PUNCT
eurjchem-1635	94	54	5h	5h	NUM
eurjchem-1635	94	55	,	,	PUNCT
eurjchem-1635	94	56	j	j	PROPN
eurjchem-1635	94	57	=	=	PROPN
eurjchem-1635	94	58	14.4	14.4	NUM
eurjchem-1635	94	59	,	,	PUNCT
eurjchem-1635	94	60	6.8	6.8	NUM
eurjchem-1635	94	61	hz	hz	NOUN
eurjchem-1635	94	62	,	,	PUNCT
eurjchem-1635	94	63	ar‐h	ar‐h	PROPN
eurjchem-1635	94	64	)	)	PUNCT
eurjchem-1635	94	65	,	,	PUNCT
eurjchem-1635	94	66	6.68‐	6.68‐	NUM
eurjchem-1635	94	67	6.62	6.62	NUM
eurjchem-1635	94	68	(	(	PUNCT
eurjchem-1635	94	69	m	m	PROPN
eurjchem-1635	94	70	,	,	PUNCT
eurjchem-1635	94	71	3h	3h	NUM
eurjchem-1635	94	72	,	,	PUNCT
eurjchem-1635	94	73	j	j	PROPN
eurjchem-1635	94	74	=	=	PROPN
eurjchem-1635	94	75	14.4	14.4	NUM
eurjchem-1635	94	76	,	,	PUNCT
eurjchem-1635	94	77	7.8	7.8	NUM
eurjchem-1635	94	78	hz	hz	NOUN
eurjchem-1635	94	79	,	,	PUNCT
eurjchem-1635	94	80	ar‐h	ar‐h	PROPN
eurjchem-1635	94	81	)	)	PUNCT
eurjchem-1635	94	82	,	,	PUNCT
eurjchem-1635	94	83	6.51	6.51	NUM
eurjchem-1635	94	84	(	(	PUNCT
eurjchem-1635	94	85	q	q	NOUN
eurjchem-1635	94	86	,	,	PUNCT
eurjchem-1635	94	87	1h	1h	NUM
eurjchem-1635	94	88	,	,	PUNCT
eurjchem-1635	94	89	j	j	PROPN
eurjchem-1635	94	90	=	=	PROPN
eurjchem-1635	94	91	12.8	12.8	NUM
eurjchem-1635	94	92	,	,	PUNCT
eurjchem-1635	94	93	6.8	6.8	NUM
eurjchem-1635	94	94	hz	hz	NOUN
eurjchem-1635	94	95	,	,	PUNCT
eurjchem-1635	94	96	ar‐h	ar‐h	NOUN
eurjchem-1635	94	97	)	)	PUNCT
eurjchem-1635	94	98	,	,	PUNCT
eurjchem-1635	94	99	4.48‐4.37	4.48‐4.37	PROPN
eurjchem-1635	94	100	(	(	PUNCT
eurjchem-1635	94	101	q	q	NOUN
eurjchem-1635	94	102	,	,	PUNCT
eurjchem-1635	94	103	2h	2h	NUM
eurjchem-1635	94	104	,	,	PUNCT
eurjchem-1635	94	105	j	j	PROPN
eurjchem-1635	94	106	=	=	SYM
eurjchem-1635	94	107	16.4	16.4	NUM
eurjchem-1635	94	108	,	,	PUNCT
eurjchem-1635	94	109	11.6	11.6	NUM
eurjchem-1635	94	110	hz	hz	NOUN
eurjchem-1635	94	111	,	,	PUNCT
eurjchem-1635	94	112	ph‐ch2	ph‐ch2	ADJ
eurjchem-1635	94	113	)	)	PUNCT
eurjchem-1635	94	114	,	,	PUNCT
eurjchem-1635	94	115	4.12	4.12	NUM
eurjchem-1635	94	116	(	(	PUNCT
eurjchem-1635	94	117	m	m	PROPN
eurjchem-1635	94	118	,	,	PUNCT
eurjchem-1635	94	119	1h	1h	NUM
eurjchem-1635	94	120	,	,	PUNCT
eurjchem-1635	94	121	ch2‐ch	ch2‐ch	NOUN
eurjchem-1635	94	122	)	)	PUNCT
eurjchem-1635	94	123	,	,	PUNCT
eurjchem-1635	94	124	3.37	3.37	NUM
eurjchem-1635	94	125	(	(	PUNCT
eurjchem-1635	94	126	m	m	PROPN
eurjchem-1635	94	127	,	,	PUNCT
eurjchem-1635	94	128	1h	1h	NUM
eurjchem-1635	94	129	,	,	PUNCT
eurjchem-1635	94	130	n‐ch2	n‐ch2	PROPN
eurjchem-1635	94	131	)	)	PUNCT
eurjchem-1635	94	132	,	,	PUNCT
eurjchem-1635	94	133	3.15‐3.12	3.15‐3.12	NUM
eurjchem-1635	94	134	(	(	PUNCT
eurjchem-1635	94	135	m	m	PROPN
eurjchem-1635	94	136	,	,	PUNCT
eurjchem-1635	94	137	1h	1h	NUM
eurjchem-1635	94	138	,	,	PUNCT
eurjchem-1635	94	139	n‐ch2	n‐ch2	PROPN
eurjchem-1635	94	140	)	)	PUNCT
eurjchem-1635	94	141	,	,	PUNCT
eurjchem-1635	94	142	3.02	3.02	NUM
eurjchem-1635	94	143	(	(	PUNCT
eurjchem-1635	94	144	t	t	PROPN
eurjchem-1635	94	145	,	,	PUNCT
eurjchem-1635	94	146	2h	2h	NUM
eurjchem-1635	94	147	,	,	PUNCT
eurjchem-1635	94	148	j	j	PROPN
eurjchem-1635	94	149	=	=	PROPN
eurjchem-1635	94	150	6	6	NUM
eurjchem-1635	94	151	hz	hz	VERB
eurjchem-1635	94	152	,	,	PUNCT
eurjchem-1635	94	153	nh‐ch2	nh‐ch2	ADJ
eurjchem-1635	94	154	)	)	PUNCT
eurjchem-1635	94	155	.	.	PUNCT
eurjchem-1635	95	1	13c	13c	NOUN
eurjchem-1635	95	2	nmr	nmr	NOUN
eurjchem-1635	95	3	(	(	PUNCT
eurjchem-1635	95	4	100	100	NUM
eurjchem-1635	95	5	mhz	mhz	NOUN
eurjchem-1635	95	6	,	,	PUNCT
eurjchem-1635	95	7	cdcl3	cdcl3	PROPN
eurjchem-1635	95	8	,	,	PUNCT
eurjchem-1635	95	9	δ	δ	PROPN
eurjchem-1635	95	10	,	,	PUNCT
eurjchem-1635	95	11	ppm	ppm	NOUN
eurjchem-1635	95	12	):	):	PUNCT
eurjchem-1635	95	13	145.12	145.12	NUM
eurjchem-1635	95	14	,	,	PUNCT
eurjchem-1635	95	15	143.11	143.11	NUM
eurjchem-1635	95	16	,	,	PUNCT
eurjchem-1635	95	17	140.38	140.38	NUM
eurjchem-1635	95	18	,	,	PUNCT
eurjchem-1635	95	19	135.36	135.36	NUM
eurjchem-1635	95	20	,	,	PUNCT
eurjchem-1635	95	21	129.2	129.2	NUM
eurjchem-1635	95	22	,	,	PUNCT
eurjchem-1635	95	23	128.78	128.78	NUM
eurjchem-1635	95	24	,	,	PUNCT
eurjchem-1635	95	25	128.12	128.12	NUM
eurjchem-1635	95	26	,	,	PUNCT
eurjchem-1635	95	27	127.66	127.66	NUM
eurjchem-1635	95	28	,	,	PUNCT
eurjchem-1635	95	29	127.11	127.11	NUM
eurjchem-1635	95	30	,	,	PUNCT
eurjchem-1635	95	31	127.10	127.10	NUM
eurjchem-1635	95	32	,	,	PUNCT
eurjchem-1635	95	33	127.01	127.01	NUM
eurjchem-1635	95	34	,	,	PUNCT
eurjchem-1635	95	35	126.12	126.12	NUM
eurjchem-1635	95	36	,	,	PUNCT
eurjchem-1635	95	37	125.11	125.11	NUM
eurjchem-1635	95	38	,	,	PUNCT
eurjchem-1635	95	39	125.10	125.10	NUM
eurjchem-1635	95	40	,	,	PUNCT
eurjchem-1635	95	41	115.12	115.12	NUM
eurjchem-1635	95	42	,	,	PUNCT
eurjchem-1635	95	43	115.10	115.10	NUM
eurjchem-1635	95	44	,	,	PUNCT
eurjchem-1635	95	45	110.22	110.22	NUM
eurjchem-1635	95	46	,	,	PUNCT
eurjchem-1635	95	47	110.14	110.14	NUM
eurjchem-1635	95	48	,	,	PUNCT
eurjchem-1635	95	49	80.30	80.30	NUM
eurjchem-1635	95	50	,	,	PUNCT
eurjchem-1635	95	51	60.34	60.34	NUM
eurjchem-1635	95	52	,	,	PUNCT
eurjchem-1635	95	53	55.12	55.12	NUM
eurjchem-1635	95	54	,	,	PUNCT
eurjchem-1635	95	55	43.15	43.15	NUM
eurjchem-1635	95	56	.	.	PUNCT
eurjchem-1635	96	1	ms	ms	NOUN
eurjchem-1635	96	2	(	(	PUNCT
eurjchem-1635	96	3	ei	ei	PROPN
eurjchem-1635	96	4	,	,	PUNCT
eurjchem-1635	96	5	m	m	PROPN
eurjchem-1635	96	6	/	/	SYM
eurjchem-1635	96	7	z	z	PROPN
eurjchem-1635	96	8	(	(	PUNCT
eurjchem-1635	96	9	%	%	NOUN
eurjchem-1635	96	10	)	)	PUNCT
eurjchem-1635	96	11	):	):	PUNCT
eurjchem-1635	96	12	395	395	NUM
eurjchem-1635	96	13	(	(	PUNCT
eurjchem-1635	96	14	m+h	m+h	PROPN
eurjchem-1635	96	15	)	)	PUNCT
eurjchem-1635	96	16	.	.	PUNCT
eurjchem-1635	97	1	hplc	hplc	NOUN
eurjchem-1635	97	2	:	:	PUNCT
eurjchem-1635	97	3	purity	purity	NOUN
eurjchem-1635	97	4	=	=	SYM
eurjchem-1635	98	1	98.0	98.0	NUM
eurjchem-1635	98	2	%	%	NOUN
eurjchem-1635	98	3	,	,	PUNCT
eurjchem-1635	98	4	r.t	r.t	PROPN
eurjchem-1635	98	5	.	.	PUNCT
eurjchem-1635	98	6	=	=	NOUN
eurjchem-1635	98	7	7.98	7.98	NUM
eurjchem-1635	98	8	min	min	NOUN
eurjchem-1635	98	9	.	.	PROPN
eurjchem-1635	98	10	n‐((4‐benzyl‐3	n‐((4‐benzyl‐3	PROPN
eurjchem-1635	98	11	,	,	PUNCT
eurjchem-1635	98	12	4‐dihydro‐2h‐benzo[b][1	4‐dihydro‐2h‐benzo[b][1	NOUN
eurjchem-1635	98	13	,	,	PUNCT
eurjchem-1635	98	14	4]oxazin‐2‐yl	4]oxazin‐2‐yl	NUM
eurjchem-1635	98	15	)	)	PUNCT
eurjchem-1635	98	16	methyl)‐4‐methylbenzenesulfonamide	methyl)‐4‐methylbenzenesulfonamide	PROPN
eurjchem-1635	98	17	(	(	PUNCT
eurjchem-1635	98	18	4b	4b	PROPN
eurjchem-1635	98	19	):	):	PUNCT
eurjchem-1635	98	20	color	color	NOUN
eurjchem-1635	98	21	:	:	PUNCT
eurjchem-1635	98	22	white	white	ADJ
eurjchem-1635	98	23	.	.	PUNCT
eurjchem-1635	99	1	yield	yield	NOUN
eurjchem-1635	99	2	:	:	PUNCT
eurjchem-1635	99	3	86	86	NUM
eurjchem-1635	99	4	%	%	NOUN
eurjchem-1635	99	5	.	.	PUNCT
eurjchem-1635	100	1	m.p	m.p	PROPN
eurjchem-1635	100	2	.	.	PROPN
eurjchem-1635	100	3	:	:	PUNCT
eurjchem-1635	101	1	183‐184	183‐184	NUM
eurjchem-1635	101	2	°	°	ADP
eurjchem-1635	101	3	c	c	PROPN
eurjchem-1635	101	4	.	.	PUNCT
eurjchem-1635	101	5	1h	1h	NUM
eurjchem-1635	101	6	nmr	nmr	NOUN
eurjchem-1635	101	7	(	(	PUNCT
eurjchem-1635	101	8	400	400	NUM
eurjchem-1635	101	9	mhz	mhz	NOUN
eurjchem-1635	101	10	,	,	PUNCT
eurjchem-1635	101	11	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	101	12	,	,	PUNCT
eurjchem-1635	101	13	δ	δ	PROPN
eurjchem-1635	101	14	,	,	PUNCT
eurjchem-1635	101	15	ppm	ppm	NUM
eurjchem-1635	101	16	):	):	PUNCT
eurjchem-1635	101	17	7.88‐7.85	7.88‐7.85	NUM
eurjchem-1635	101	18	(	(	PUNCT
eurjchem-1635	101	19	t	t	PROPN
eurjchem-1635	101	20	,	,	PUNCT
eurjchem-1635	101	21	1h	1h	NUM
eurjchem-1635	101	22	,	,	PUNCT
eurjchem-1635	101	23	j	j	PROPN
eurjchem-1635	101	24	=	=	SYM
eurjchem-1635	101	25	6	6	NUM
eurjchem-1635	101	26	hz	hz	NOUN
eurjchem-1635	101	27	,	,	PUNCT
eurjchem-1635	101	28	nh	nh	PROPN
eurjchem-1635	101	29	)	)	PUNCT
eurjchem-1635	101	30	,	,	PUNCT
eurjchem-1635	101	31	7.70‐7.68	7.70‐7.68	NUM
eurjchem-1635	101	32	(	(	PUNCT
eurjchem-1635	101	33	d	d	NOUN
eurjchem-1635	101	34	,	,	PUNCT
eurjchem-1635	101	35	2h	2h	NUM
eurjchem-1635	101	36	,	,	PUNCT
eurjchem-1635	101	37	j	j	PROPN
eurjchem-1635	101	38	=	=	SYM
eurjchem-1635	101	39	8	8	NUM
eurjchem-1635	101	40	hz	hz	NOUN
eurjchem-1635	101	41	,	,	PUNCT
eurjchem-1635	101	42	ar‐h	ar‐h	PROPN
eurjchem-1635	101	43	)	)	PUNCT
eurjchem-1635	101	44	,	,	PUNCT
eurjchem-1635	101	45	7.39‐7.37	7.39‐7.37	PROPN
eurjchem-1635	101	46	(	(	PUNCT
eurjchem-1635	101	47	d	d	PROPN
eurjchem-1635	101	48	,	,	PUNCT
eurjchem-1635	101	49	2h	2h	NUM
eurjchem-1635	101	50	,	,	PUNCT
eurjchem-1635	101	51	j	j	PROPN
eurjchem-1635	102	1	=	=	SYM
eurjchem-1635	102	2	7.8	7.8	NUM
eurjchem-1635	102	3	hz	hz	NOUN
eurjchem-1635	102	4	,	,	PUNCT
eurjchem-1635	102	5	ar‐h	ar‐h	PROPN
eurjchem-1635	102	6	)	)	PUNCT
eurjchem-1635	102	7	,	,	PUNCT
eurjchem-1635	102	8	7.34‐7.30	7.34‐7.30	NUM
eurjchem-1635	102	9	(	(	PUNCT
eurjchem-1635	102	10	m	m	PROPN
eurjchem-1635	102	11	,	,	PUNCT
eurjchem-1635	102	12	2h	2h	NUM
eurjchem-1635	102	13	,	,	PUNCT
eurjchem-1635	102	14	ar‐h	ar‐h	NOUN
eurjchem-1635	102	15	)	)	PUNCT
eurjchem-1635	102	16	,	,	PUNCT
eurjchem-1635	102	17	7.26‐7.24	7.26‐7.24	NUM
eurjchem-1635	102	18	(	(	PUNCT
eurjchem-1635	102	19	m	m	PROPN
eurjchem-1635	102	20	,	,	PUNCT
eurjchem-1635	102	21	3h	3h	NUM
eurjchem-1635	102	22	,	,	PUNCT
eurjchem-1635	102	23	ar‐h	ar‐h	NOUN
eurjchem-1635	102	24	)	)	PUNCT
eurjchem-1635	102	25	,	,	PUNCT
eurjchem-1635	102	26	6.88‐6.63	6.88‐6.63	PROPN
eurjchem-1635	102	27	(	(	PUNCT
eurjchem-1635	102	28	m	m	PROPN
eurjchem-1635	102	29	,	,	PUNCT
eurjchem-1635	102	30	3h	3h	NUM
eurjchem-1635	102	31	,	,	PUNCT
eurjchem-1635	102	32	ar‐h	ar‐h	NOUN
eurjchem-1635	102	33	)	)	PUNCT
eurjchem-1635	102	34	,	,	PUNCT
eurjchem-1635	102	35	6.51	6.51	NUM
eurjchem-1635	102	36	(	(	PUNCT
eurjchem-1635	102	37	t	t	PROPN
eurjchem-1635	102	38	,	,	PUNCT
eurjchem-1635	102	39	1h	1h	NUM
eurjchem-1635	102	40	,	,	PUNCT
eurjchem-1635	102	41	j	j	PROPN
eurjchem-1635	102	42	=	=	SYM
eurjchem-1635	102	43	7.8	7.8	NUM
eurjchem-1635	102	44	hz	hz	NOUN
eurjchem-1635	102	45	,	,	PUNCT
eurjchem-1635	102	46	ar‐h	ar‐h	NOUN
eurjchem-1635	102	47	)	)	PUNCT
eurjchem-1635	102	48	,	,	PUNCT
eurjchem-1635	102	49	4.48‐4.37	4.48‐4.37	PROPN
eurjchem-1635	102	50	(	(	PUNCT
eurjchem-1635	102	51	q	q	NOUN
eurjchem-1635	102	52	,	,	PUNCT
eurjchem-1635	102	53	2h	2h	NUM
eurjchem-1635	102	54	,	,	PUNCT
eurjchem-1635	102	55	j	j	PROPN
eurjchem-1635	102	56	=	=	SYM
eurjchem-1635	102	57	24.8	24.8	NUM
eurjchem-1635	102	58	,	,	PUNCT
eurjchem-1635	102	59	8.0	8.0	NUM
eurjchem-1635	102	60	hz	hz	VERB
eurjchem-1635	102	61	,	,	PUNCT
eurjchem-1635	102	62	ph‐ch2	ph‐ch2	ADJ
eurjchem-1635	102	63	)	)	PUNCT
eurjchem-1635	102	64	,	,	PUNCT
eurjchem-1635	102	65	4.12	4.12	NUM
eurjchem-1635	102	66	(	(	PUNCT
eurjchem-1635	102	67	m	m	PROPN
eurjchem-1635	102	68	,	,	PUNCT
eurjchem-1635	102	69	1h	1h	NUM
eurjchem-1635	102	70	,	,	PUNCT
eurjchem-1635	102	71	ch2‐ch	ch2‐ch	NOUN
eurjchem-1635	102	72	)	)	PUNCT
eurjchem-1635	102	73	,	,	PUNCT
eurjchem-1635	102	74	3.37	3.37	NUM
eurjchem-1635	102	75	(	(	PUNCT
eurjchem-1635	102	76	m	m	PROPN
eurjchem-1635	102	77	,	,	PUNCT
eurjchem-1635	102	78	1h	1h	NUM
eurjchem-1635	102	79	,	,	PUNCT
eurjchem-1635	102	80	n‐ch2	n‐ch2	PROPN
eurjchem-1635	102	81	)	)	PUNCT
eurjchem-1635	102	82	,	,	PUNCT
eurjchem-1635	102	83	3.17‐3.12	3.17‐3.12	NUM
eurjchem-1635	102	84	(	(	PUNCT
eurjchem-1635	102	85	m	m	PROPN
eurjchem-1635	102	86	,	,	PUNCT
eurjchem-1635	102	87	1h	1h	NUM
eurjchem-1635	102	88	,	,	PUNCT
eurjchem-1635	102	89	n‐	n‐	NOUN
eurjchem-1635	102	90	ch2	ch2	PROPN
eurjchem-1635	102	91	)	)	PUNCT
eurjchem-1635	102	92	,	,	PUNCT
eurjchem-1635	102	93	2.99	2.99	NUM
eurjchem-1635	102	94	(	(	PUNCT
eurjchem-1635	102	95	t	t	PROPN
eurjchem-1635	102	96	,	,	PUNCT
eurjchem-1635	102	97	2h	2h	NUM
eurjchem-1635	102	98	,	,	PUNCT
eurjchem-1635	102	99	j	j	PROPN
eurjchem-1635	102	100	=	=	PROPN
eurjchem-1635	102	101	6	6	NUM
eurjchem-1635	102	102	hz	hz	VERB
eurjchem-1635	102	103	,	,	PUNCT
eurjchem-1635	102	104	nh‐ch2	nh‐ch2	ADJ
eurjchem-1635	102	105	)	)	PUNCT
eurjchem-1635	102	106	,	,	PUNCT
eurjchem-1635	102	107	2.37	2.37	NUM
eurjchem-1635	102	108	(	(	PUNCT
eurjchem-1635	102	109	s	s	PROPN
eurjchem-1635	102	110	,	,	PUNCT
eurjchem-1635	102	111	3h	3h	NUM
eurjchem-1635	102	112	,	,	PUNCT
eurjchem-1635	102	113	ph‐ch3	ph‐ch3	NOUN
eurjchem-1635	102	114	)	)	PUNCT
eurjchem-1635	102	115	.	.	PUNCT
eurjchem-1635	103	1	13c	13c	NOUN
eurjchem-1635	103	2	nmr	nmr	NOUN
eurjchem-1635	103	3	(	(	PUNCT
eurjchem-1635	103	4	100	100	NUM
eurjchem-1635	103	5	mhz	mhz	NOUN
eurjchem-1635	103	6	,	,	PUNCT
eurjchem-1635	103	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	103	8	,	,	PUNCT
eurjchem-1635	103	9	δ	δ	PROPN
eurjchem-1635	103	10	,	,	PUNCT
eurjchem-1635	103	11	ppm	ppm	NOUN
eurjchem-1635	103	12	):	):	PUNCT
eurjchem-1635	103	13	149.8	149.8	NUM
eurjchem-1635	103	14	,	,	PUNCT
eurjchem-1635	103	15	145.5	145.5	NUM
eurjchem-1635	103	16	,	,	PUNCT
eurjchem-1635	103	17	138.7	138.7	NUM
eurjchem-1635	103	18	,	,	PUNCT
eurjchem-1635	103	19	135.1	135.1	NUM
eurjchem-1635	103	20	,	,	PUNCT
eurjchem-1635	103	21	133.4	133.4	NUM
eurjchem-1635	103	22	,	,	PUNCT
eurjchem-1635	103	23	132.8	132.8	NUM
eurjchem-1635	103	24	,	,	PUNCT
eurjchem-1635	103	25	130	130	NUM
eurjchem-1635	103	26	,	,	PUNCT
eurjchem-1635	103	27	129.8	129.8	NUM
eurjchem-1635	103	28	,	,	PUNCT
eurjchem-1635	103	29	129.2	129.2	NUM
eurjchem-1635	103	30	,	,	PUNCT
eurjchem-1635	103	31	127.2	127.2	NUM
eurjchem-1635	103	32	,	,	PUNCT
eurjchem-1635	103	33	126.0	126.0	NUM
eurjchem-1635	103	34	,	,	PUNCT
eurjchem-1635	103	35	124.9	124.9	NUM
eurjchem-1635	103	36	,	,	PUNCT
eurjchem-1635	103	37	124.1	124.1	NUM
eurjchem-1635	103	38	,	,	PUNCT
eurjchem-1635	103	39	123	123	NUM
eurjchem-1635	103	40	,	,	PUNCT
eurjchem-1635	103	41	80.3	80.3	NUM
eurjchem-1635	103	42	,	,	PUNCT
eurjchem-1635	103	43	60.34	60.34	NUM
eurjchem-1635	103	44	,	,	PUNCT
eurjchem-1635	103	45	55.12	55.12	NUM
eurjchem-1635	103	46	,	,	PUNCT
eurjchem-1635	103	47	43.18	43.18	NUM
eurjchem-1635	103	48	,	,	PUNCT
eurjchem-1635	103	49	24.12	24.12	NUM
eurjchem-1635	103	50	.	.	PUNCT
eurjchem-1635	104	1	ms	ms	NOUN
eurjchem-1635	104	2	(	(	PUNCT
eurjchem-1635	104	3	ei	ei	PROPN
eurjchem-1635	104	4	,	,	PUNCT
eurjchem-1635	104	5	m	m	PROPN
eurjchem-1635	104	6	/	/	SYM
eurjchem-1635	104	7	z	z	PROPN
eurjchem-1635	104	8	(	(	PUNCT
eurjchem-1635	104	9	%	%	NOUN
eurjchem-1635	104	10	)	)	PUNCT
eurjchem-1635	104	11	):	):	PUNCT
eurjchem-1635	104	12	409	409	NUM
eurjchem-1635	105	1	[	[	X
eurjchem-1635	105	2	m+h	m+h	NOUN
eurjchem-1635	105	3	]	]	PUNCT
eurjchem-1635	105	4	.	.	PUNCT
eurjchem-1635	106	1	hplc	hplc	NOUN
eurjchem-1635	106	2	:	:	PUNCT
eurjchem-1635	106	3	purity	purity	NOUN
eurjchem-1635	106	4	=	=	SYM
eurjchem-1635	106	5	97.4	97.4	NUM
eurjchem-1635	106	6	%	%	NOUN
eurjchem-1635	106	7	,	,	PUNCT
eurjchem-1635	106	8	r.t	r.t	PROPN
eurjchem-1635	106	9	.	.	PUNCT
eurjchem-1635	106	10	=	=	NOUN
eurjchem-1635	106	11	8.18	8.18	NUM
eurjchem-1635	106	12	min	min	NOUN
eurjchem-1635	106	13	.	.	PROPN
eurjchem-1635	106	14	n‐((4‐benzyl‐3	n‐((4‐benzyl‐3	PROPN
eurjchem-1635	106	15	,	,	PUNCT
eurjchem-1635	106	16	4‐dihydro‐2h‐benzo[b][1	4‐dihydro‐2h‐benzo[b][1	NOUN
eurjchem-1635	106	17	,	,	PUNCT
eurjchem-1635	106	18	4]oxazin‐2‐yl	4]oxazin‐2‐yl	NUM
eurjchem-1635	106	19	)	)	PUNCT
eurjchem-1635	106	20	methyl)‐4‐chlorobenzenesulfonamide	methyl)‐4‐chlorobenzenesulfonamide	NOUN
eurjchem-1635	106	21	(	(	PUNCT
eurjchem-1635	106	22	4c	4c	NOUN
eurjchem-1635	106	23	):	):	PUNCT
eurjchem-1635	106	24	color	color	NOUN
eurjchem-1635	106	25	:	:	PUNCT
eurjchem-1635	106	26	white	white	ADJ
eurjchem-1635	106	27	.	.	PUNCT
eurjchem-1635	107	1	yield	yield	NOUN
eurjchem-1635	107	2	:	:	PUNCT
eurjchem-1635	107	3	88	88	NUM
eurjchem-1635	107	4	%	%	NOUN
eurjchem-1635	107	5	.	.	PUNCT
eurjchem-1635	108	1	m.p	m.p	PROPN
eurjchem-1635	108	2	.	.	PROPN
eurjchem-1635	108	3	:	:	PUNCT
eurjchem-1635	109	1	207‐208	207‐208	NUM
eurjchem-1635	109	2	°	°	PROPN
eurjchem-1635	109	3	c	c	PROPN
eurjchem-1635	109	4	.	.	PUNCT
eurjchem-1635	109	5	1h	1h	NUM
eurjchem-1635	109	6	nmr	nmr	NOUN
eurjchem-1635	109	7	(	(	PUNCT
eurjchem-1635	109	8	400	400	NUM
eurjchem-1635	109	9	mhz	mhz	NOUN
eurjchem-1635	109	10	,	,	PUNCT
eurjchem-1635	109	11	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	109	12	,	,	PUNCT
eurjchem-1635	109	13	δ	δ	PROPN
eurjchem-1635	109	14	,	,	PUNCT
eurjchem-1635	109	15	ppm	ppm	NUM
eurjchem-1635	109	16	):	):	PUNCT
eurjchem-1635	109	17	8.08	8.08	NUM
eurjchem-1635	109	18	(	(	PUNCT
eurjchem-1635	109	19	br	br	PROPN
eurjchem-1635	109	20	,	,	PUNCT
eurjchem-1635	109	21	1h	1h	NUM
eurjchem-1635	109	22	,	,	PUNCT
eurjchem-1635	109	23	nh	nh	PROPN
eurjchem-1635	109	24	)	)	PUNCT
eurjchem-1635	109	25	,	,	PUNCT
eurjchem-1635	109	26	7.82‐7.80	7.82‐7.80	NUM
eurjchem-1635	109	27	(	(	PUNCT
eurjchem-1635	109	28	d	d	NOUN
eurjchem-1635	109	29	,	,	PUNCT
eurjchem-1635	109	30	2h	2h	NUM
eurjchem-1635	109	31	,	,	PUNCT
eurjchem-1635	109	32	j	j	PROPN
eurjchem-1635	109	33	=	=	PROPN
eurjchem-1635	109	34	8.4	8.4	NUM
eurjchem-1635	109	35	hz	hz	NOUN
eurjchem-1635	109	36	,	,	PUNCT
eurjchem-1635	109	37	ar‐h	ar‐h	NOUN
eurjchem-1635	109	38	)	)	PUNCT
eurjchem-1635	109	39	,	,	PUNCT
eurjchem-1635	109	40	7.67‐7.44	7.67‐7.44	NUM
eurjchem-1635	109	41	(	(	PUNCT
eurjchem-1635	109	42	d	d	NOUN
eurjchem-1635	109	43	,	,	PUNCT
eurjchem-1635	109	44	2h	2h	NUM
eurjchem-1635	109	45	,	,	PUNCT
eurjchem-1635	109	46	j	j	PROPN
eurjchem-1635	109	47	=	=	PROPN
eurjchem-1635	109	48	8.4	8.4	NUM
eurjchem-1635	109	49	hz	hz	NOUN
eurjchem-1635	109	50	,	,	PUNCT
eurjchem-1635	109	51	ar‐h	ar‐h	PROPN
eurjchem-1635	109	52	)	)	PUNCT
eurjchem-1635	109	53	,	,	PUNCT
eurjchem-1635	109	54	7.34‐7.24	7.34‐7.24	NUM
eurjchem-1635	109	55	(	(	PUNCT
eurjchem-1635	109	56	m	m	PROPN
eurjchem-1635	109	57	,	,	PUNCT
eurjchem-1635	109	58	5h	5h	NUM
eurjchem-1635	109	59	,	,	PUNCT
eurjchem-1635	109	60	ar‐h	ar‐h	NOUN
eurjchem-1635	109	61	)	)	PUNCT
eurjchem-1635	109	62	,	,	PUNCT
eurjchem-1635	109	63	6.70‐6.60	6.70‐6.60	NUM
eurjchem-1635	109	64	(	(	PUNCT
eurjchem-1635	109	65	m	m	PROPN
eurjchem-1635	109	66	,	,	PUNCT
eurjchem-1635	109	67	3h	3h	NUM
eurjchem-1635	109	68	,	,	PUNCT
eurjchem-1635	109	69	ar‐h	ar‐h	NOUN
eurjchem-1635	109	70	)	)	PUNCT
eurjchem-1635	109	71	,	,	PUNCT
eurjchem-1635	109	72	6.51	6.51	NUM
eurjchem-1635	109	73	(	(	PUNCT
eurjchem-1635	109	74	t	t	PROPN
eurjchem-1635	109	75	,	,	PUNCT
eurjchem-1635	109	76	1h	1h	NUM
eurjchem-1635	109	77	,	,	PUNCT
eurjchem-1635	109	78	j	j	PROPN
eurjchem-1635	109	79	=	=	SYM
eurjchem-1635	109	80	7.2	7.2	NUM
eurjchem-1635	109	81	hz	hz	NOUN
eurjchem-1635	109	82	,	,	PUNCT
eurjchem-1635	109	83	ar‐h	ar‐h	NOUN
eurjchem-1635	109	84	)	)	PUNCT
eurjchem-1635	109	85	,	,	PUNCT
eurjchem-1635	109	86	4.48‐4.37	4.48‐4.37	PROPN
eurjchem-1635	109	87	(	(	PUNCT
eurjchem-1635	109	88	q	q	NOUN
eurjchem-1635	109	89	,	,	PUNCT
eurjchem-1635	109	90	2h	2h	NUM
eurjchem-1635	109	91	,	,	PUNCT
eurjchem-1635	109	92	j	j	PROPN
eurjchem-1635	109	93	=	=	PROPN
eurjchem-1635	109	94	16.2	16.2	NUM
eurjchem-1635	109	95	,	,	PUNCT
eurjchem-1635	109	96	11.2	11.2	NUM
eurjchem-1635	109	97	hz	hz	NOUN
eurjchem-1635	109	98	,	,	PUNCT
eurjchem-1635	109	99	ph‐ch2	ph‐ch2	ADJ
eurjchem-1635	109	100	)	)	PUNCT
eurjchem-1635	109	101	,	,	PUNCT
eurjchem-1635	109	102	4.12	4.12	NUM
eurjchem-1635	109	103	(	(	PUNCT
eurjchem-1635	109	104	m	m	PROPN
eurjchem-1635	109	105	,	,	PUNCT
eurjchem-1635	109	106	1h	1h	NUM
eurjchem-1635	109	107	,	,	PUNCT
eurjchem-1635	109	108	ch2‐ch	ch2‐ch	NOUN
eurjchem-1635	109	109	)	)	PUNCT
eurjchem-1635	109	110	,	,	PUNCT
eurjchem-1635	109	111	3.37	3.37	NUM
eurjchem-1635	109	112	(	(	PUNCT
eurjchem-1635	109	113	m	m	PROPN
eurjchem-1635	109	114	,	,	PUNCT
eurjchem-1635	109	115	1h	1h	NUM
eurjchem-1635	109	116	,	,	PUNCT
eurjchem-1635	109	117	n‐	n‐	NOUN
eurjchem-1635	109	118	ch2	ch2	PROPN
eurjchem-1635	109	119	)	)	PUNCT
eurjchem-1635	109	120	,	,	PUNCT
eurjchem-1635	109	121	3.30‐3.18	3.30‐3.18	NUM
eurjchem-1635	109	122	(	(	PUNCT
eurjchem-1635	109	123	m	m	PROPN
eurjchem-1635	109	124	,	,	PUNCT
eurjchem-1635	109	125	1h	1h	NUM
eurjchem-1635	109	126	,	,	PUNCT
eurjchem-1635	109	127	n‐ch2	n‐ch2	PROPN
eurjchem-1635	109	128	)	)	PUNCT
eurjchem-1635	109	129	,	,	PUNCT
eurjchem-1635	109	130	3.04	3.04	NUM
eurjchem-1635	109	131	(	(	PUNCT
eurjchem-1635	109	132	d	d	NOUN
eurjchem-1635	109	133	,	,	PUNCT
eurjchem-1635	109	134	2h	2h	NUM
eurjchem-1635	109	135	,	,	PUNCT
eurjchem-1635	109	136	j	j	PROPN
eurjchem-1635	109	137	=	=	SYM
eurjchem-1635	109	138	5.2	5.2	NUM
eurjchem-1635	109	139	hz	hz	NOUN
eurjchem-1635	109	140	,	,	PUNCT
eurjchem-1635	109	141	nh‐ch2	nh‐ch2	ADJ
eurjchem-1635	109	142	)	)	PUNCT
eurjchem-1635	109	143	.	.	PUNCT
eurjchem-1635	110	1	13c	13c	NOUN
eurjchem-1635	110	2	nmr	nmr	NOUN
eurjchem-1635	110	3	(	(	PUNCT
eurjchem-1635	110	4	100	100	NUM
eurjchem-1635	110	5	mhz	mhz	NOUN
eurjchem-1635	110	6	,	,	PUNCT
eurjchem-1635	110	7	cdcl3	cdcl3	PROPN
eurjchem-1635	110	8	,	,	PUNCT
eurjchem-1635	110	9	δ	δ	PROPN
eurjchem-1635	110	10	,	,	PUNCT
eurjchem-1635	110	11	ppm	ppm	NOUN
eurjchem-1635	110	12	):	):	PUNCT
eurjchem-1635	110	13	145.12	145.12	NUM
eurjchem-1635	110	14	,	,	PUNCT
eurjchem-1635	110	15	143.11	143.11	NUM
eurjchem-1635	110	16	,	,	PUNCT
eurjchem-1635	110	17	140.38	140.38	NUM
eurjchem-1635	110	18	,	,	PUNCT
eurjchem-1635	110	19	137.68	137.68	NUM
eurjchem-1635	110	20	,	,	PUNCT
eurjchem-1635	110	21	135.36	135.36	NUM
eurjchem-1635	110	22	,	,	PUNCT
eurjchem-1635	110	23	129.2	129.2	NUM
eurjchem-1635	110	24	,	,	PUNCT
eurjchem-1635	110	25	128.78	128.78	NUM
eurjchem-1635	110	26	,	,	PUNCT
eurjchem-1635	110	27	127.66	127.66	NUM
eurjchem-1635	110	28	,	,	PUNCT
eurjchem-1635	110	29	127.21	127.21	NUM
eurjchem-1635	110	30	,	,	PUNCT
eurjchem-1635	110	31	127.11	127.11	NUM
eurjchem-1635	110	32	,	,	PUNCT
eurjchem-1635	110	33	127.08	127.08	NUM
eurjchem-1635	110	34	,	,	PUNCT
eurjchem-1635	110	35	126.12	126.12	NUM
eurjchem-1635	110	36	,	,	PUNCT
eurjchem-1635	110	37	125.11	125.11	NUM
eurjchem-1635	110	38	,	,	PUNCT
eurjchem-1635	110	39	125.18	125.18	NUM
eurjchem-1635	110	40	,	,	PUNCT
eurjchem-1635	110	41	115.12	115.12	NUM
eurjchem-1635	110	42	,	,	PUNCT
eurjchem-1635	110	43	115.10	115.10	NUM
eurjchem-1635	110	44	,	,	PUNCT
eurjchem-1635	110	45	110.22	110.22	NUM
eurjchem-1635	110	46	,	,	PUNCT
eurjchem-1635	110	47	110.24	110.24	NUM
eurjchem-1635	110	48	,	,	PUNCT
eurjchem-1635	110	49	80.30	80.30	NUM
eurjchem-1635	110	50	,	,	PUNCT
eurjchem-1635	110	51	60.34	60.34	NUM
eurjchem-1635	110	52	,	,	PUNCT
eurjchem-1635	110	53	55.12	55.12	NUM
eurjchem-1635	110	54	,	,	PUNCT
eurjchem-1635	110	55	43.14	43.14	NUM
eurjchem-1635	110	56	.	.	PUNCT
eurjchem-1635	111	1	ms	ms	NOUN
eurjchem-1635	111	2	(	(	PUNCT
eurjchem-1635	111	3	ei	ei	PROPN
eurjchem-1635	111	4	,	,	PUNCT
eurjchem-1635	111	5	m	m	PROPN
eurjchem-1635	111	6	/	/	SYM
eurjchem-1635	111	7	z	z	PROPN
eurjchem-1635	111	8	(	(	PUNCT
eurjchem-1635	111	9	%	%	NOUN
eurjchem-1635	111	10	)	)	PUNCT
eurjchem-1635	111	11	):	):	PUNCT
eurjchem-1635	111	12	429	429	NUM
eurjchem-1635	112	1	[	[	X
eurjchem-1635	112	2	m+h	m+h	NOUN
eurjchem-1635	112	3	]	]	X
eurjchem-1635	112	4	.	.	PUNCT
eurjchem-1635	113	1	hplc	hplc	NOUN
eurjchem-1635	113	2	:	:	PUNCT
eurjchem-1635	113	3	purity	purity	NOUN
eurjchem-1635	113	4	=	=	SYM
eurjchem-1635	113	5	95.4	95.4	NUM
eurjchem-1635	113	6	%	%	NOUN
eurjchem-1635	113	7	,	,	PUNCT
eurjchem-1635	113	8	r.t	r.t	PROPN
eurjchem-1635	113	9	.	.	PUNCT
eurjchem-1635	113	10	=	=	NOUN
eurjchem-1635	113	11	8.18	8.18	NUM
eurjchem-1635	113	12	min	min	NOUN
eurjchem-1635	113	13	.	.	PROPN
eurjchem-1635	113	14	n‐((4‐benzyl‐3	n‐((4‐benzyl‐3	PROPN
eurjchem-1635	113	15	,	,	PUNCT
eurjchem-1635	113	16	4‐dihydro‐2h‐benzo[b][1	4‐dihydro‐2h‐benzo[b][1	NOUN
eurjchem-1635	113	17	,	,	PUNCT
eurjchem-1635	113	18	4]oxazin‐2‐yl	4]oxazin‐2‐yl	NUM
eurjchem-1635	113	19	)	)	PUNCT
eurjchem-1635	113	20	methyl)‐4‐(trifluoromethyl)benzenesulfonamide	methyl)‐4‐(trifluoromethyl)benzenesulfonamide	PROPN
eurjchem-1635	113	21	(	(	PUNCT
eurjchem-1635	113	22	4d	4d	NUM
eurjchem-1635	113	23	):	):	PUNCT
eurjchem-1635	113	24	color	color	NOUN
eurjchem-1635	113	25	:	:	PUNCT
eurjchem-1635	113	26	white	white	ADJ
eurjchem-1635	113	27	.	.	PUNCT
eurjchem-1635	114	1	yield	yield	NOUN
eurjchem-1635	114	2	:	:	PUNCT
eurjchem-1635	114	3	89	89	NUM
eurjchem-1635	114	4	%	%	NOUN
eurjchem-1635	114	5	.	.	PUNCT
eurjchem-1635	115	1	m.p	m.p	PROPN
eurjchem-1635	115	2	.	.	PROPN
eurjchem-1635	115	3	:	:	PUNCT
eurjchem-1635	116	1	214‐215	214‐215	NUM
eurjchem-1635	116	2	°	°	PROPN
eurjchem-1635	116	3	c	c	PROPN
eurjchem-1635	116	4	.	.	PUNCT
eurjchem-1635	116	5	1h	1h	NUM
eurjchem-1635	116	6	nmr	nmr	NOUN
eurjchem-1635	116	7	(	(	PUNCT
eurjchem-1635	116	8	400	400	NUM
eurjchem-1635	116	9	mhz	mhz	NOUN
eurjchem-1635	116	10	,	,	PUNCT
eurjchem-1635	116	11	dmso‐	dmso‐	NUM
eurjchem-1635	116	12	d6	d6	NOUN
eurjchem-1635	116	13	,	,	PUNCT
eurjchem-1635	116	14	δ	δ	PROPN
eurjchem-1635	116	15	,	,	PUNCT
eurjchem-1635	116	16	ppm	ppm	NUM
eurjchem-1635	116	17	):	):	PUNCT
eurjchem-1635	116	18	8.08	8.08	NUM
eurjchem-1635	116	19	(	(	PUNCT
eurjchem-1635	116	20	br	br	PROPN
eurjchem-1635	116	21	,	,	PUNCT
eurjchem-1635	116	22	1h	1h	NUM
eurjchem-1635	116	23	,	,	PUNCT
eurjchem-1635	116	24	nh	nh	PROPN
eurjchem-1635	116	25	)	)	PUNCT
eurjchem-1635	116	26	,	,	PUNCT
eurjchem-1635	116	27	7.83‐7.61	7.83‐7.61	NUM
eurjchem-1635	116	28	(	(	PUNCT
eurjchem-1635	116	29	d	d	NOUN
eurjchem-1635	116	30	,	,	PUNCT
eurjchem-1635	116	31	2h	2h	NUM
eurjchem-1635	116	32	,	,	PUNCT
eurjchem-1635	116	33	j	j	PROPN
eurjchem-1635	116	34	=	=	PROPN
eurjchem-1635	116	35	8.4	8.4	NUM
eurjchem-1635	116	36	hz	hz	NOUN
eurjchem-1635	116	37	,	,	PUNCT
eurjchem-1635	116	38	ar‐	ar‐	PROPN
eurjchem-1635	116	39	h	h	NOUN
eurjchem-1635	116	40	)	)	PUNCT
eurjchem-1635	116	41	,	,	PUNCT
eurjchem-1635	116	42	7.66‐7.44	7.66‐7.44	NUM
eurjchem-1635	116	43	(	(	PUNCT
eurjchem-1635	116	44	d	d	PROPN
eurjchem-1635	116	45	,	,	PUNCT
eurjchem-1635	116	46	2h	2h	NUM
eurjchem-1635	116	47	,	,	PUNCT
eurjchem-1635	116	48	j	j	PROPN
eurjchem-1635	117	1	=	=	PROPN
eurjchem-1635	117	2	8.4	8.4	NUM
eurjchem-1635	117	3	hz	hz	NOUN
eurjchem-1635	117	4	,	,	PUNCT
eurjchem-1635	117	5	ar‐h	ar‐h	PROPN
eurjchem-1635	117	6	)	)	PUNCT
eurjchem-1635	117	7	,	,	PUNCT
eurjchem-1635	117	8	7.34‐7.29	7.34‐7.29	NUM
eurjchem-1635	117	9	(	(	PUNCT
eurjchem-1635	117	10	m	m	PROPN
eurjchem-1635	117	11	,	,	PUNCT
eurjchem-1635	117	12	5h	5h	NUM
eurjchem-1635	117	13	,	,	PUNCT
eurjchem-1635	117	14	ar‐h	ar‐h	NOUN
eurjchem-1635	117	15	)	)	PUNCT
eurjchem-1635	117	16	,	,	PUNCT
eurjchem-1635	117	17	6.71‐6.61	6.71‐6.61	NUM
eurjchem-1635	117	18	(	(	PUNCT
eurjchem-1635	117	19	m	m	PROPN
eurjchem-1635	117	20	,	,	PUNCT
eurjchem-1635	117	21	3h	3h	NUM
eurjchem-1635	117	22	,	,	PUNCT
eurjchem-1635	117	23	ar‐h	ar‐h	NOUN
eurjchem-1635	117	24	)	)	PUNCT
eurjchem-1635	117	25	,	,	PUNCT
eurjchem-1635	117	26	6.51	6.51	NUM
eurjchem-1635	117	27	(	(	PUNCT
eurjchem-1635	117	28	m	m	PROPN
eurjchem-1635	117	29	,	,	PUNCT
eurjchem-1635	117	30	1h	1h	NUM
eurjchem-1635	117	31	,	,	PUNCT
eurjchem-1635	117	32	ar‐h	ar‐h	NOUN
eurjchem-1635	117	33	)	)	PUNCT
eurjchem-1635	117	34	,	,	PUNCT
eurjchem-1635	117	35	4.48‐4.37	4.48‐4.37	PROPN
eurjchem-1635	117	36	(	(	PUNCT
eurjchem-1635	117	37	q	q	NOUN
eurjchem-1635	117	38	,	,	PUNCT
eurjchem-1635	117	39	2h	2h	NUM
eurjchem-1635	117	40	,	,	PUNCT
eurjchem-1635	117	41	j	j	PROPN
eurjchem-1635	117	42	=	=	PROPN
eurjchem-1635	117	43	17.2	17.2	NUM
eurjchem-1635	117	44	,	,	PUNCT
eurjchem-1635	117	45	11.0	11.0	NUM
eurjchem-1635	117	46	hz	hz	NOUN
eurjchem-1635	117	47	,	,	PUNCT
eurjchem-1635	117	48	ph‐ch2	ph‐ch2	ADJ
eurjchem-1635	117	49	)	)	PUNCT
eurjchem-1635	117	50	,	,	PUNCT
eurjchem-1635	117	51	4.10	4.10	NUM
eurjchem-1635	117	52	(	(	PUNCT
eurjchem-1635	117	53	m	m	PROPN
eurjchem-1635	117	54	,	,	PUNCT
eurjchem-1635	117	55	1h	1h	NUM
eurjchem-1635	117	56	,	,	PUNCT
eurjchem-1635	117	57	ch2‐ch	ch2‐ch	NOUN
eurjchem-1635	117	58	)	)	PUNCT
eurjchem-1635	117	59	,	,	PUNCT
eurjchem-1635	117	60	3.37	3.37	NUM
eurjchem-1635	117	61	(	(	PUNCT
eurjchem-1635	117	62	m	m	PROPN
eurjchem-1635	117	63	,	,	PUNCT
eurjchem-1635	117	64	1h	1h	NUM
eurjchem-1635	117	65	,	,	PUNCT
eurjchem-1635	117	66	n‐	n‐	NOUN
eurjchem-1635	117	67	ch2	ch2	PROPN
eurjchem-1635	117	68	)	)	PUNCT
eurjchem-1635	117	69	,	,	PUNCT
eurjchem-1635	117	70	3.30‐3.18	3.30‐3.18	NUM
eurjchem-1635	117	71	(	(	PUNCT
eurjchem-1635	117	72	m	m	PROPN
eurjchem-1635	117	73	,	,	PUNCT
eurjchem-1635	117	74	1h	1h	NUM
eurjchem-1635	117	75	,	,	PUNCT
eurjchem-1635	117	76	n‐ch2	n‐ch2	PROPN
eurjchem-1635	117	77	)	)	PUNCT
eurjchem-1635	117	78	,	,	PUNCT
eurjchem-1635	117	79	3.06	3.06	NUM
eurjchem-1635	117	80	(	(	PUNCT
eurjchem-1635	117	81	t	t	PROPN
eurjchem-1635	117	82	,	,	PUNCT
eurjchem-1635	117	83	2h	2h	NUM
eurjchem-1635	117	84	,	,	PUNCT
eurjchem-1635	117	85	j	j	PROPN
eurjchem-1635	117	86	=	=	PROPN
eurjchem-1635	117	87	5.4	5.4	NUM
eurjchem-1635	117	88	hz	hz	NOUN
eurjchem-1635	117	89	,	,	PUNCT
eurjchem-1635	117	90	nh‐ch2	nh‐ch2	ADJ
eurjchem-1635	117	91	)	)	PUNCT
eurjchem-1635	117	92	.	.	PUNCT
eurjchem-1635	118	1	13c	13c	NOUN
eurjchem-1635	118	2	nmr	nmr	NOUN
eurjchem-1635	118	3	(	(	PUNCT
eurjchem-1635	118	4	100	100	NUM
eurjchem-1635	118	5	mhz	mhz	NOUN
eurjchem-1635	118	6	,	,	PUNCT
eurjchem-1635	118	7	cdcl3	cdcl3	PROPN
eurjchem-1635	118	8	,	,	PUNCT
eurjchem-1635	118	9	δ	δ	PROPN
eurjchem-1635	118	10	,	,	PUNCT
eurjchem-1635	118	11	ppm	ppm	NOUN
eurjchem-1635	118	12	):	):	PUNCT
eurjchem-1635	118	13	145.12	145.12	NUM
eurjchem-1635	118	14	,	,	PUNCT
eurjchem-1635	118	15	143.11	143.11	NUM
eurjchem-1635	118	16	,	,	PUNCT
eurjchem-1635	118	17	140.38	140.38	NUM
eurjchem-1635	118	18	,	,	PUNCT
eurjchem-1635	118	19	135.36	135.36	NUM
eurjchem-1635	118	20	,	,	PUNCT
eurjchem-1635	118	21	134.44	134.44	NUM
eurjchem-1635	118	22	,	,	PUNCT
eurjchem-1635	118	23	129.24	129.24	NUM
eurjchem-1635	118	24	,	,	PUNCT
eurjchem-1635	118	25	128.88	128.88	NUM
eurjchem-1635	118	26	,	,	PUNCT
eurjchem-1635	118	27	128.12	128.12	NUM
eurjchem-1635	118	28	,	,	PUNCT
eurjchem-1635	118	29	127.66	127.66	NUM
eurjchem-1635	118	30	,	,	PUNCT
eurjchem-1635	118	31	127.11	127.11	NUM
eurjchem-1635	118	32	,	,	PUNCT
eurjchem-1635	118	33	127.14	127.14	NUM
eurjchem-1635	118	34	,	,	PUNCT
eurjchem-1635	118	35	127.01	127.01	NUM
eurjchem-1635	118	36	,	,	PUNCT
eurjchem-1635	118	37	126.12	126.12	NUM
eurjchem-1635	118	38	,	,	PUNCT
eurjchem-1635	118	39	125.11	125.11	NUM
eurjchem-1635	118	40	,	,	PUNCT
eurjchem-1635	118	41	125.10	125.10	NUM
eurjchem-1635	118	42	,	,	PUNCT
eurjchem-1635	118	43	115.12	115.12	NUM
eurjchem-1635	118	44	,	,	PUNCT
eurjchem-1635	118	45	115.10	115.10	NUM
eurjchem-1635	118	46	,	,	PUNCT
eurjchem-1635	118	47	110.22	110.22	NUM
eurjchem-1635	118	48	,	,	PUNCT
eurjchem-1635	118	49	110.14	110.14	NUM
eurjchem-1635	118	50	,	,	PUNCT
eurjchem-1635	118	51	80.30	80.30	NUM
eurjchem-1635	118	52	,	,	PUNCT
eurjchem-1635	118	53	60.34	60.34	NUM
eurjchem-1635	118	54	,	,	PUNCT
eurjchem-1635	118	55	55.22	55.22	NUM
eurjchem-1635	118	56	,	,	PUNCT
eurjchem-1635	118	57	43.14	43.14	NUM
eurjchem-1635	118	58	.	.	PUNCT
eurjchem-1635	119	1	ms	ms	NOUN
eurjchem-1635	119	2	(	(	PUNCT
eurjchem-1635	119	3	ei	ei	PROPN
eurjchem-1635	119	4	,	,	PUNCT
eurjchem-1635	119	5	m	m	PROPN
eurjchem-1635	119	6	/	/	SYM
eurjchem-1635	119	7	z	z	PROPN
eurjchem-1635	119	8	(	(	PUNCT
eurjchem-1635	119	9	%	%	NOUN
eurjchem-1635	119	10	)	)	PUNCT
eurjchem-1635	119	11	):	):	PUNCT
eurjchem-1635	119	12	462	462	NUM
eurjchem-1635	120	1	[	[	X
eurjchem-1635	120	2	m+h	m+h	NOUN
eurjchem-1635	120	3	]	]	PUNCT
eurjchem-1635	120	4	.	.	PUNCT
eurjchem-1635	121	1	hplc	hplc	NOUN
eurjchem-1635	121	2	:	:	PUNCT
eurjchem-1635	121	3	purity	purity	NOUN
eurjchem-1635	121	4	=	=	SYM
eurjchem-1635	121	5	97.4	97.4	NUM
eurjchem-1635	121	6	%	%	NOUN
eurjchem-1635	121	7	,	,	PUNCT
eurjchem-1635	121	8	r.t	r.t	PROPN
eurjchem-1635	121	9	.	.	PUNCT
eurjchem-1635	121	10	=	=	PROPN
eurjchem-1635	121	11	8.28	8.28	NUM
eurjchem-1635	121	12	min	min	NOUN
eurjchem-1635	121	13	.	.	PROPN
eurjchem-1635	121	14	n‐((4‐benzyl‐3	n‐((4‐benzyl‐3	PROPN
eurjchem-1635	121	15	,	,	PUNCT
eurjchem-1635	121	16	4‐dihydro‐2h‐benzo[b][1	4‐dihydro‐2h‐benzo[b][1	NOUN
eurjchem-1635	121	17	,	,	PUNCT
eurjchem-1635	121	18	4]oxazin‐2‐yl	4]oxazin‐2‐yl	NUM
eurjchem-1635	121	19	)	)	PUNCT
eurjchem-1635	121	20	methyl)methanesulfonamide	methyl)methanesulfonamide	PROPN
eurjchem-1635	121	21	(	(	PUNCT
eurjchem-1635	121	22	4e	4e	NOUN
eurjchem-1635	121	23	):	):	PUNCT
eurjchem-1635	121	24	color	color	NOUN
eurjchem-1635	121	25	:	:	PUNCT
eurjchem-1635	121	26	yellow	yellow	ADJ
eurjchem-1635	121	27	.	.	PUNCT
eurjchem-1635	122	1	yield	yield	NOUN
eurjchem-1635	122	2	:	:	PUNCT
eurjchem-1635	122	3	81	81	NUM
eurjchem-1635	122	4	%	%	NOUN
eurjchem-1635	122	5	.	.	PUNCT
eurjchem-1635	123	1	m.p	m.p	PROPN
eurjchem-1635	123	2	.	.	PROPN
eurjchem-1635	123	3	:	:	PUNCT
eurjchem-1635	124	1	135‐136	135‐136	NUM
eurjchem-1635	124	2	°	°	PROPN
eurjchem-1635	124	3	c	c	PROPN
eurjchem-1635	124	4	.	.	PUNCT
eurjchem-1635	125	1	1h	1h	NUM
eurjchem-1635	125	2	nmr	nmr	NOUN
eurjchem-1635	125	3	(	(	PUNCT
eurjchem-1635	125	4	400	400	NUM
eurjchem-1635	125	5	mhz	mhz	NOUN
eurjchem-1635	125	6	,	,	PUNCT
eurjchem-1635	125	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	125	8	,	,	PUNCT
eurjchem-1635	125	9	δ	δ	PROPN
eurjchem-1635	125	10	,	,	PUNCT
eurjchem-1635	125	11	ppm	ppm	NOUN
eurjchem-1635	125	12	):	):	PUNCT
eurjchem-1635	125	13	7.35‐	7.35‐	NUM
eurjchem-1635	125	14	7.23	7.23	NUM
eurjchem-1635	125	15	(	(	PUNCT
eurjchem-1635	125	16	m	m	PROPN
eurjchem-1635	125	17	,	,	PUNCT
eurjchem-1635	125	18	6h	6h	NUM
eurjchem-1635	125	19	,	,	PUNCT
eurjchem-1635	125	20	ar‐h	ar‐h	PROPN
eurjchem-1635	125	21	)	)	PUNCT
eurjchem-1635	125	22	,	,	PUNCT
eurjchem-1635	125	23	6.74‐6.67	6.74‐6.67	NUM
eurjchem-1635	125	24	(	(	PUNCT
eurjchem-1635	125	25	m	m	PROPN
eurjchem-1635	125	26	,	,	PUNCT
eurjchem-1635	125	27	3h	3h	NUM
eurjchem-1635	125	28	,	,	PUNCT
eurjchem-1635	125	29	ar‐h	ar‐h	NOUN
eurjchem-1635	125	30	)	)	PUNCT
eurjchem-1635	125	31	,	,	PUNCT
eurjchem-1635	125	32	6.54	6.54	NUM
eurjchem-1635	125	33	(	(	PUNCT
eurjchem-1635	125	34	t	t	PROPN
eurjchem-1635	125	35	,	,	PUNCT
eurjchem-1635	125	36	1h	1h	NUM
eurjchem-1635	125	37	,	,	PUNCT
eurjchem-1635	125	38	j	j	PROPN
eurjchem-1635	125	39	=	=	PROPN
eurjchem-1635	125	40	6.4	6.4	NUM
eurjchem-1635	125	41	hz	hz	NOUN
eurjchem-1635	125	42	,	,	PUNCT
eurjchem-1635	125	43	nh	nh	PROPN
eurjchem-1635	125	44	)	)	PUNCT
eurjchem-1635	125	45	,	,	PUNCT
eurjchem-1635	125	46	4.53‐4.42	4.53‐4.42	NUM
eurjchem-1635	125	47	(	(	PUNCT
eurjchem-1635	125	48	q	q	NOUN
eurjchem-1635	125	49	,	,	PUNCT
eurjchem-1635	125	50	2h	2h	NUM
eurjchem-1635	125	51	,	,	PUNCT
eurjchem-1635	125	52	j	j	PROPN
eurjchem-1635	125	53	=	=	NOUN
eurjchem-1635	125	54	15.6	15.6	NUM
eurjchem-1635	125	55	,	,	PUNCT
eurjchem-1635	125	56	8.8	8.8	NUM
eurjchem-1635	125	57	hz	hz	NOUN
eurjchem-1635	125	58	,	,	PUNCT
eurjchem-1635	125	59	ph‐ch2	ph‐ch2	ADJ
eurjchem-1635	125	60	)	)	PUNCT
eurjchem-1635	125	61	,	,	PUNCT
eurjchem-1635	125	62	4.20	4.20	NUM
eurjchem-1635	125	63	(	(	PUNCT
eurjchem-1635	125	64	m	m	PROPN
eurjchem-1635	125	65	,	,	PUNCT
eurjchem-1635	125	66	1h	1h	NUM
eurjchem-1635	125	67	,	,	PUNCT
eurjchem-1635	125	68	ch2‐ch	ch2‐ch	NOUN
eurjchem-1635	125	69	)	)	PUNCT
eurjchem-1635	125	70	,	,	PUNCT
eurjchem-1635	125	71	3.42‐3.37	3.42‐3.37	NUM
eurjchem-1635	125	72	(	(	PUNCT
eurjchem-1635	125	73	m	m	PROPN
eurjchem-1635	125	74	,	,	PUNCT
eurjchem-1635	125	75	1h	1h	NUM
eurjchem-1635	125	76	,	,	PUNCT
eurjchem-1635	125	77	n‐ch2	n‐ch2	PROPN
eurjchem-1635	125	78	)	)	PUNCT
eurjchem-1635	125	79	,	,	PUNCT
eurjchem-1635	125	80	3.21‐3.16	3.21‐3.16	NUM
eurjchem-1635	125	81	(	(	PUNCT
eurjchem-1635	125	82	m	m	PROPN
eurjchem-1635	125	83	,	,	PUNCT
eurjchem-1635	125	84	3h	3h	NUM
eurjchem-1635	125	85	,	,	PUNCT
eurjchem-1635	125	86	n‐ch2	n‐ch2	PROPN
eurjchem-1635	125	87	,	,	PUNCT
eurjchem-1635	125	88	nh‐ch2	nh‐ch2	NOUN
eurjchem-1635	125	89	)	)	PUNCT
eurjchem-1635	125	90	,	,	PUNCT
eurjchem-1635	125	91	2.94	2.94	NUM
eurjchem-1635	125	92	(	(	PUNCT
eurjchem-1635	125	93	s	s	PROPN
eurjchem-1635	125	94	,	,	PUNCT
eurjchem-1635	125	95	3h	3h	NUM
eurjchem-1635	125	96	,	,	PUNCT
eurjchem-1635	125	97	s‐ch3	s‐ch3	PROPN
eurjchem-1635	125	98	)	)	PUNCT
eurjchem-1635	125	99	.	.	PUNCT
eurjchem-1635	126	1	13c	13c	NOUN
eurjchem-1635	126	2	nmr	nmr	NOUN
eurjchem-1635	126	3	(	(	PUNCT
eurjchem-1635	126	4	100	100	NUM
eurjchem-1635	126	5	mhz	mhz	NOUN
eurjchem-1635	126	6	,	,	PUNCT
eurjchem-1635	126	7	cdcl3	cdcl3	PROPN
eurjchem-1635	126	8	,	,	PUNCT
eurjchem-1635	126	9	δ	δ	PROPN
eurjchem-1635	126	10	,	,	PUNCT
eurjchem-1635	126	11	ppm	ppm	NOUN
eurjchem-1635	126	12	):	):	PUNCT
eurjchem-1635	126	13	145.12	145.12	NUM
eurjchem-1635	126	14	,	,	PUNCT
eurjchem-1635	126	15	143.11	143.11	NUM
eurjchem-1635	126	16	,	,	PUNCT
eurjchem-1635	126	17	140.38	140.38	NUM
eurjchem-1635	126	18	,	,	PUNCT
eurjchem-1635	126	19	135.36	135.36	NUM
eurjchem-1635	126	20	,	,	PUNCT
eurjchem-1635	126	21	128.78	128.78	NUM
eurjchem-1635	126	22	,	,	PUNCT
eurjchem-1635	126	23	128.12	128.12	NUM
eurjchem-1635	126	24	,	,	PUNCT
eurjchem-1635	126	25	127.66	127.66	NUM
eurjchem-1635	126	26	,	,	PUNCT
eurjchem-1635	126	27	127.01	127.01	NUM
eurjchem-1635	126	28	,	,	PUNCT
eurjchem-1635	126	29	126.12	126.12	NUM
eurjchem-1635	126	30	,	,	PUNCT
eurjchem-1635	126	31	115.12	115.12	NUM
eurjchem-1635	126	32	,	,	PUNCT
eurjchem-1635	126	33	115.10	115.10	NUM
eurjchem-1635	126	34	,	,	PUNCT
eurjchem-1635	126	35	110.22	110.22	NUM
eurjchem-1635	126	36	,	,	PUNCT
eurjchem-1635	126	37	110.14	110.14	NUM
eurjchem-1635	126	38	,	,	PUNCT
eurjchem-1635	126	39	80.3	80.3	NUM
eurjchem-1635	126	40	,	,	PUNCT
eurjchem-1635	126	41	60.34	60.34	NUM
eurjchem-1635	126	42	,	,	PUNCT
eurjchem-1635	126	43	55.12	55.12	NUM
eurjchem-1635	126	44	,	,	PUNCT
eurjchem-1635	126	45	43.15	43.15	NUM
eurjchem-1635	126	46	,	,	PUNCT
eurjchem-1635	126	47	41.21	41.21	NUM
eurjchem-1635	126	48	.	.	PUNCT
eurjchem-1635	127	1	ms	ms	NOUN
eurjchem-1635	127	2	(	(	PUNCT
eurjchem-1635	127	3	ei	ei	PROPN
eurjchem-1635	127	4	,	,	PUNCT
eurjchem-1635	127	5	m	m	PROPN
eurjchem-1635	127	6	/	/	SYM
eurjchem-1635	127	7	z	z	PROPN
eurjchem-1635	127	8	(	(	PUNCT
eurjchem-1635	127	9	%	%	NOUN
eurjchem-1635	127	10	)	)	PUNCT
eurjchem-1635	127	11	):	):	PUNCT
eurjchem-1635	127	12	333	333	NUM
eurjchem-1635	127	13	[	[	X
eurjchem-1635	127	14	m+h	m+h	NOUN
eurjchem-1635	127	15	]	]	PUNCT
eurjchem-1635	127	16	.	.	PUNCT
eurjchem-1635	128	1	hplc	hplc	NOUN
eurjchem-1635	128	2	:	:	PUNCT
eurjchem-1635	128	3	purity	purity	NOUN
eurjchem-1635	128	4	=	=	SYM
eurjchem-1635	128	5	97.4	97.4	NUM
eurjchem-1635	128	6	%	%	NOUN
eurjchem-1635	128	7	,	,	PUNCT
eurjchem-1635	128	8	r.t	r.t	PROPN
eurjchem-1635	128	9	.	.	PUNCT
eurjchem-1635	128	10	=	=	PROPN
eurjchem-1635	128	11	7.20	7.20	NUM
eurjchem-1635	128	12	min	min	NOUN
eurjchem-1635	128	13	.	.	PROPN
eurjchem-1635	128	14	2.2.5	2.2.5	NUM
eurjchem-1635	128	15	.	.	PUNCT
eurjchem-1635	129	1	synthesis	synthesis	NOUN
eurjchem-1635	129	2	of	of	ADP
eurjchem-1635	129	3	2‐(chloromethyl)‐3,4‐dihydro‐2h‐benzo	2‐(chloromethyl)‐3,4‐dihydro‐2h‐benzo	NUM
eurjchem-1635	129	4	[	[	X
eurjchem-1635	129	5	b][1,4]oxazine	b][1,4]oxazine	X
eurjchem-1635	129	6	(	(	PUNCT
eurjchem-1635	129	7	5	5	NUM
eurjchem-1635	129	8	)	)	PUNCT
eurjchem-1635	129	9	to	to	ADP
eurjchem-1635	129	10	a	a	DET
eurjchem-1635	129	11	stirred	stir	VERB
eurjchem-1635	129	12	solution	solution	NOUN
eurjchem-1635	129	13	of	of	ADP
eurjchem-1635	129	14	2‐aminophenol	2‐aminophenol	NUM
eurjchem-1635	129	15	(	(	PUNCT
eurjchem-1635	129	16	5	5	NUM
eurjchem-1635	129	17	g	g	NOUN
eurjchem-1635	129	18	,	,	PUNCT
eurjchem-1635	129	19	45.8	45.8	NUM
eurjchem-1635	129	20	mmol	mmol	NOUN
eurjchem-1635	129	21	)	)	PUNCT
eurjchem-1635	129	22	was	be	AUX
eurjchem-1635	129	23	dissolved	dissolve	VERB
eurjchem-1635	129	24	in	in	ADP
eurjchem-1635	129	25	toluene	toluene	NOUN
eurjchem-1635	129	26	(	(	PUNCT
eurjchem-1635	129	27	50	50	NUM
eurjchem-1635	129	28	ml	ml	NOUN
eurjchem-1635	129	29	)	)	PUNCT
eurjchem-1635	129	30	then	then	ADV
eurjchem-1635	129	31	added	add	VERB
eurjchem-1635	129	32	cesium	cesium	NOUN
eurjchem-1635	129	33	carbo‐	carbo‐	PROPN
eurjchem-1635	129	34	nate	nate	PROPN
eurjchem-1635	129	35	(	(	PUNCT
eurjchem-1635	129	36	18.7	18.7	NUM
eurjchem-1635	129	37	g	g	NOUN
eurjchem-1635	129	38	,	,	PUNCT
eurjchem-1635	129	39	57.4	57.4	NUM
eurjchem-1635	129	40	mmol	mmol	NOUN
eurjchem-1635	129	41	)	)	PUNCT
eurjchem-1635	129	42	.	.	PUNCT
eurjchem-1635	130	1	stirred	stir	VERB
eurjchem-1635	130	2	reaction	reaction	NOUN
eurjchem-1635	130	3	mixture	mixture	NOUN
eurjchem-1635	130	4	at	at	ADP
eurjchem-1635	130	5	60	60	NUM
eurjchem-1635	130	6	°	°	ADP
eurjchem-1635	130	7	c	c	NOUN
eurjchem-1635	130	8	for	for	ADP
eurjchem-1635	130	9	0.5	0.5	NUM
eurjchem-1635	130	10	h	h	NOUN
eurjchem-1635	130	11	then	then	ADV
eurjchem-1635	130	12	added	add	VERB
eurjchem-1635	130	13	2‐chloromethylacrylo	2‐chloromethylacrylo	NUM
eurjchem-1635	130	14	nitrile	nitrile	NOUN
eurjchem-1635	130	15	(	(	PUNCT
eurjchem-1635	130	16	5.79	5.79	NUM
eurjchem-1635	130	17	g	g	NOUN
eurjchem-1635	130	18	,	,	PUNCT
eurjchem-1635	130	19	57.4	57.4	NUM
eurjchem-1635	130	20	mmol	mmol	NOUN
eurjchem-1635	130	21	)	)	PUNCT
eurjchem-1635	130	22	and	and	CCONJ
eurjchem-1635	130	23	heat	heat	NOUN
eurjchem-1635	130	24	reaction	reaction	NOUN
eurjchem-1635	130	25	mixture	mixture	NOUN
eurjchem-1635	130	26	at	at	ADP
eurjchem-1635	130	27	110	110	NUM
eurjchem-1635	130	28	°	°	NOUN
eurjchem-1635	130	29	c	c	NOUN
eurjchem-1635	130	30	for	for	ADP
eurjchem-1635	130	31	4	4	NUM
eurjchem-1635	130	32	h.	h.	NOUN
eurjchem-1635	130	33	after	after	SCONJ
eurjchem-1635	130	34	completion	completion	NOUN
eurjchem-1635	130	35	the	the	DET
eurjchem-1635	130	36	raection	raection	NOUN
eurjchem-1635	130	37	,	,	PUNCT
eurjchem-1635	130	38	we	we	PRON
eurjchem-1635	130	39	evaporated	evaporate	VERB
eurjchem-1635	130	40	reaction	reaction	NOUN
eurjchem-1635	130	41	mixture	mixture	NOUN
eurjchem-1635	130	42	under	under	ADP
eurjchem-1635	130	43	reduced	reduce	VERB
eurjchem-1635	130	44	pressure	pressure	NOUN
eurjchem-1635	130	45	to	to	PART
eurjchem-1635	130	46	obtain	obtain	VERB
eurjchem-1635	130	47	crude	crude	ADJ
eurjchem-1635	130	48	yellow	yellow	ADJ
eurjchem-1635	130	49	gummy	gummy	ADJ
eurjchem-1635	130	50	mass	mass	NOUN
eurjchem-1635	130	51	.	.	PUNCT
eurjchem-1635	131	1	added	add	VERB
eurjchem-1635	131	2	h2o	h2o	PROPN
eurjchem-1635	131	3	(	(	PUNCT
eurjchem-1635	131	4	50	50	NUM
eurjchem-1635	131	5	ml	ml	NOUN
eurjchem-1635	131	6	)	)	PUNCT
eurjchem-1635	131	7	and	and	CCONJ
eurjchem-1635	131	8	extracted	extract	VERB
eurjchem-1635	131	9	it	it	PRON
eurjchem-1635	131	10	with	with	ADP
eurjchem-1635	131	11	etoac	etoac	ADJ
eurjchem-1635	131	12	(	(	PUNCT
eurjchem-1635	131	13	2	2	NUM
eurjchem-1635	131	14	×	×	NOUN
eurjchem-1635	131	15	50	50	NUM
eurjchem-1635	131	16	ml	ml	NOUN
eurjchem-1635	131	17	)	)	PUNCT
eurjchem-1635	131	18	.	.	PUNCT
eurjchem-1635	132	1	the	the	DET
eurjchem-1635	132	2	organic	organic	ADJ
eurjchem-1635	132	3	layer	layer	NOUN
eurjchem-1635	132	4	was	be	AUX
eurjchem-1635	132	5	separated	separate	VERB
eurjchem-1635	132	6	,	,	PUNCT
eurjchem-1635	132	7	washed	wash	VERB
eurjchem-1635	132	8	with	with	ADP
eurjchem-1635	132	9	h2o	h2o	PROPN
eurjchem-1635	132	10	(	(	PUNCT
eurjchem-1635	132	11	25	25	NUM
eurjchem-1635	132	12	ml	ml	NOUN
eurjchem-1635	132	13	)	)	PUNCT
eurjchem-1635	132	14	and	and	CCONJ
eurjchem-1635	132	15	brine	brine	NOUN
eurjchem-1635	132	16	(	(	PUNCT
eurjchem-1635	132	17	25	25	NUM
eurjchem-1635	132	18	ml	ml	NOUN
eurjchem-1635	132	19	)	)	PUNCT
eurjchem-1635	132	20	,	,	PUNCT
eurjchem-1635	132	21	dried	dry	VERB
eurjchem-1635	132	22	over	over	ADP
eurjchem-1635	132	23	anhydrous	anhydrous	ADJ
eurjchem-1635	132	24	na2so4	na2so4	NOUN
eurjchem-1635	132	25	and	and	CCONJ
eurjchem-1635	132	26	concent‐	concent‐	NOUN
eurjchem-1635	132	27	rated	rate	VERB
eurjchem-1635	132	28	in	in	ADP
eurjchem-1635	132	29	vacuum	vacuum	NOUN
eurjchem-1635	132	30	.	.	PUNCT
eurjchem-1635	133	1	purification	purification	NOUN
eurjchem-1635	133	2	of	of	ADP
eurjchem-1635	133	3	crude	crude	NOUN
eurjchem-1635	133	4	done	do	VERB
eurjchem-1635	133	5	by	by	ADP
eurjchem-1635	133	6	silica	silica	NOUN
eurjchem-1635	133	7	gel	gel	NOUN
eurjchem-1635	133	8	(	(	PUNCT
eurjchem-1635	133	9	100‐	100‐	NUM
eurjchem-1635	133	10	200	200	NUM
eurjchem-1635	133	11	mesh	mesh	NOUN
eurjchem-1635	133	12	)	)	PUNCT
eurjchem-1635	133	13	column	column	NOUN
eurjchem-1635	133	14	chromatography	chromatography	NOUN
eurjchem-1635	133	15	by	by	ADP
eurjchem-1635	133	16	using	use	VERB
eurjchem-1635	133	17	etoac	etoac	ADJ
eurjchem-1635	133	18	:	:	PUNCT
eurjchem-1635	133	19	hexane	hexane	NOUN
eurjchem-1635	133	20	(	(	PUNCT
eurjchem-1635	133	21	90:10	90:10	NUM
eurjchem-1635	133	22	,	,	PUNCT
eurjchem-1635	133	23	v	v	NOUN
eurjchem-1635	133	24	:	:	SYM
eurjchem-1635	133	25	v	v	NOUN
eurjchem-1635	133	26	)	)	PUNCT
eurjchem-1635	133	27	to	to	PART
eurjchem-1635	133	28	obtain	obtain	VERB
eurjchem-1635	133	29	3,4‐dihydro‐2h‐benzo[b][1,4]oxazine‐2‐	3,4‐dihydro‐2h‐benzo[b][1,4]oxazine‐2‐	NUM
eurjchem-1635	133	30	carbonitrile	carbonitrile	NOUN
eurjchem-1635	133	31	(	(	PUNCT
eurjchem-1635	133	32	5	5	NUM
eurjchem-1635	133	33	)	)	PUNCT
eurjchem-1635	133	34	(	(	PUNCT
eurjchem-1635	133	35	scheme	scheme	NOUN
eurjchem-1635	133	36	2	2	NUM
eurjchem-1635	133	37	)	)	PUNCT
eurjchem-1635	133	38	.	.	PUNCT
eurjchem-1635	134	1	color	color	NOUN
eurjchem-1635	134	2	:	:	PUNCT
eurjchem-1635	134	3	yellow	yellow	ADJ
eurjchem-1635	134	4	.	.	PUNCT
eurjchem-1635	135	1	yield	yield	NOUN
eurjchem-1635	135	2	:	:	PUNCT
eurjchem-1635	135	3	87	87	NUM
eurjchem-1635	135	4	%	%	NOUN
eurjchem-1635	135	5	.	.	PUNCT
eurjchem-1635	136	1	ms	ms	NOUN
eurjchem-1635	136	2	(	(	PUNCT
eurjchem-1635	136	3	ei	ei	PROPN
eurjchem-1635	136	4	,	,	PUNCT
eurjchem-1635	136	5	m	m	PROPN
eurjchem-1635	136	6	/	/	SYM
eurjchem-1635	136	7	z	z	PROPN
eurjchem-1635	136	8	(	(	PUNCT
eurjchem-1635	136	9	%	%	NOUN
eurjchem-1635	136	10	)	)	PUNCT
eurjchem-1635	136	11	):	):	PUNCT
eurjchem-1635	137	1	184	184	NUM
eurjchem-1635	137	2	[	[	X
eurjchem-1635	137	3	m+h]+	m+h]+	X
eurjchem-1635	137	4	.	.	PROPN
eurjchem-1635	138	1	1h	1h	NUM
eurjchem-1635	138	2	nmr	nmr	NOUN
eurjchem-1635	138	3	(	(	PUNCT
eurjchem-1635	138	4	400	400	NUM
eurjchem-1635	138	5	mhz	mhz	NOUN
eurjchem-1635	138	6	,	,	PUNCT
eurjchem-1635	138	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	138	8	,	,	PUNCT
eurjchem-1635	138	9	δ	δ	PROPN
eurjchem-1635	138	10	,	,	PUNCT
eurjchem-1635	138	11	ppm	ppm	NUM
eurjchem-1635	138	12	):	):	PUNCT
eurjchem-1635	138	13	pawar	pawar	PROPN
eurjchem-1635	138	14	et	et	PROPN
eurjchem-1635	138	15	al	al	PROPN
eurjchem-1635	138	16	.	.	PUNCT
eurjchem-1635	138	17	/	/	SYM
eurjchem-1635	138	18	european	european	PROPN
eurjchem-1635	138	19	journal	journal	PROPN
eurjchem-1635	138	20	of	of	ADP
eurjchem-1635	138	21	chemistry	chemistry	NOUN
eurjchem-1635	138	22	8	8	NUM
eurjchem-1635	138	23	(	(	PUNCT
eurjchem-1635	138	24	4	4	NUM
eurjchem-1635	138	25	)	)	PUNCT
eurjchem-1635	138	26	(	(	PUNCT
eurjchem-1635	138	27	2017	2017	NUM
eurjchem-1635	138	28	)	)	PUNCT
eurjchem-1635	138	29	384‐390	384‐390	NUM
eurjchem-1635	138	30	387	387	NUM
eurjchem-1635	138	31	6.80‐6.71	6.80‐6.71	NUM
eurjchem-1635	138	32	(	(	PUNCT
eurjchem-1635	138	33	m	m	PROPN
eurjchem-1635	138	34	,	,	PUNCT
eurjchem-1635	138	35	2h	2h	NUM
eurjchem-1635	138	36	,	,	PUNCT
eurjchem-1635	138	37	ar‐h	ar‐h	NOUN
eurjchem-1635	138	38	)	)	PUNCT
eurjchem-1635	138	39	,	,	PUNCT
eurjchem-1635	138	40	6.60‐6.54	6.60‐6.54	NUM
eurjchem-1635	138	41	(	(	PUNCT
eurjchem-1635	138	42	m	m	PROPN
eurjchem-1635	138	43	,	,	PUNCT
eurjchem-1635	138	44	2h	2h	NUM
eurjchem-1635	138	45	,	,	PUNCT
eurjchem-1635	138	46	ar‐h	ar‐h	NOUN
eurjchem-1635	138	47	)	)	PUNCT
eurjchem-1635	138	48	,	,	PUNCT
eurjchem-1635	138	49	5.31	5.31	NUM
eurjchem-1635	138	50	(	(	PUNCT
eurjchem-1635	138	51	m	m	PROPN
eurjchem-1635	138	52	,	,	PUNCT
eurjchem-1635	138	53	1h	1h	NUM
eurjchem-1635	138	54	,	,	PUNCT
eurjchem-1635	138	55	ch2‐ch	ch2‐ch	NOUN
eurjchem-1635	138	56	)	)	PUNCT
eurjchem-1635	138	57	,	,	PUNCT
eurjchem-1635	138	58	4.01	4.01	NUM
eurjchem-1635	138	59	(	(	PUNCT
eurjchem-1635	138	60	br	br	PROPN
eurjchem-1635	138	61	,	,	PUNCT
eurjchem-1635	138	62	1h	1h	NUM
eurjchem-1635	138	63	,	,	PUNCT
eurjchem-1635	138	64	nh	nh	PROPN
eurjchem-1635	138	65	)	)	PUNCT
eurjchem-1635	138	66	,	,	PUNCT
eurjchem-1635	138	67	3.83‐3.61	3.83‐3.61	NUM
eurjchem-1635	138	68	(	(	PUNCT
eurjchem-1635	138	69	m	m	PROPN
eurjchem-1635	138	70	,	,	PUNCT
eurjchem-1635	138	71	4h	4h	NOUN
eurjchem-1635	138	72	,	,	PUNCT
eurjchem-1635	138	73	ch‐ch2	ch‐ch2	PROPN
eurjchem-1635	138	74	,	,	PUNCT
eurjchem-1635	138	75	cl‐ch2	cl‐ch2	PROPN
eurjchem-1635	138	76	)	)	PUNCT
eurjchem-1635	138	77	.	.	PUNCT
eurjchem-1635	139	1	2.2.6	2.2.6	X
eurjchem-1635	139	2	.	.	PUNCT
eurjchem-1635	139	3	synthesis	synthesis	NOUN
eurjchem-1635	139	4	of	of	ADP
eurjchem-1635	139	5	2‐((benzylthio)methyl)‐3,4‐dihydro‐2h‐	2‐((benzylthio)methyl)‐3,4‐dihydro‐2h‐	NUM
eurjchem-1635	139	6	benzo[b][1,4]oxazine	benzo[b][1,4]oxazine	NOUN
eurjchem-1635	139	7	(	(	PUNCT
eurjchem-1635	139	8	6	6	NUM
eurjchem-1635	139	9	)	)	PUNCT
eurjchem-1635	139	10	to	to	ADP
eurjchem-1635	139	11	a	a	DET
eurjchem-1635	139	12	stirred	stir	VERB
eurjchem-1635	139	13	solution	solution	NOUN
eurjchem-1635	139	14	of	of	ADP
eurjchem-1635	139	15	compound	compound	NOUN
eurjchem-1635	139	16	5	5	NUM
eurjchem-1635	139	17	(	(	PUNCT
eurjchem-1635	139	18	0.36	0.36	NUM
eurjchem-1635	139	19	g	g	NOUN
eurjchem-1635	139	20	,	,	PUNCT
eurjchem-1635	139	21	2.00	2.00	NUM
eurjchem-1635	139	22	mmol	mmol	NOUN
eurjchem-1635	139	23	)	)	PUNCT
eurjchem-1635	139	24	in	in	ADP
eurjchem-1635	139	25	thf	thf	NOUN
eurjchem-1635	139	26	(	(	PUNCT
eurjchem-1635	139	27	10	10	NUM
eurjchem-1635	139	28	ml	ml	NOUN
eurjchem-1635	139	29	)	)	PUNCT
eurjchem-1635	139	30	was	be	AUX
eurjchem-1635	139	31	added	add	VERB
eurjchem-1635	139	32	naoh	naoh	NOUN
eurjchem-1635	139	33	(	(	PUNCT
eurjchem-1635	139	34	0.08	0.08	NUM
eurjchem-1635	139	35	g	g	NOUN
eurjchem-1635	139	36	,	,	PUNCT
eurjchem-1635	139	37	2.00	2.00	NUM
eurjchem-1635	139	38	mmol	mmol	NOUN
eurjchem-1635	139	39	)	)	PUNCT
eurjchem-1635	139	40	and	and	CCONJ
eurjchem-1635	139	41	mixture	mixture	NOUN
eurjchem-1635	139	42	was	be	AUX
eurjchem-1635	139	43	stirred	stir	VERB
eurjchem-1635	139	44	at	at	ADP
eurjchem-1635	139	45	room	room	NOUN
eurjchem-1635	139	46	temperature	temperature	NOUN
eurjchem-1635	139	47	for	for	ADP
eurjchem-1635	139	48	15	15	NUM
eurjchem-1635	139	49	min	min	NOUN
eurjchem-1635	139	50	.	.	PUNCT
eurjchem-1635	140	1	the	the	DET
eurjchem-1635	140	2	reaction	reaction	NOUN
eurjchem-1635	140	3	mixture	mixture	NOUN
eurjchem-1635	140	4	was	be	AUX
eurjchem-1635	140	5	cooled	cool	VERB
eurjchem-1635	140	6	to	to	ADP
eurjchem-1635	140	7	0	0	NUM
eurjchem-1635	140	8	°	°	ADP
eurjchem-1635	140	9	c	c	NOUN
eurjchem-1635	140	10	and	and	CCONJ
eurjchem-1635	140	11	phenylmethanethiol	phenylmethanethiol	PROPN
eurjchem-1635	140	12	(	(	PUNCT
eurjchem-1635	140	13	0.29	0.29	NUM
eurjchem-1635	140	14	g	g	NOUN
eurjchem-1635	140	15	,	,	PUNCT
eurjchem-1635	140	16	2.40	2.40	NUM
eurjchem-1635	140	17	mmol	mmol	NOUN
eurjchem-1635	140	18	)	)	PUNCT
eurjchem-1635	140	19	was	be	AUX
eurjchem-1635	140	20	added	add	VERB
eurjchem-1635	140	21	drop	drop	NOUN
eurjchem-1635	140	22	wise	wise	ADJ
eurjchem-1635	140	23	followed	follow	VERB
eurjchem-1635	140	24	by	by	ADP
eurjchem-1635	140	25	stirring	stir	VERB
eurjchem-1635	140	26	at	at	ADP
eurjchem-1635	140	27	80	80	NUM
eurjchem-1635	140	28	°	°	NUM
eurjchem-1635	140	29	c	c	NOUN
eurjchem-1635	140	30	for	for	ADP
eurjchem-1635	140	31	1	1	NUM
eurjchem-1635	140	32	h.	h.	NOUN
eurjchem-1635	140	33	the	the	DET
eurjchem-1635	140	34	reaction	reaction	NOUN
eurjchem-1635	140	35	was	be	AUX
eurjchem-1635	140	36	monitored	monitor	VERB
eurjchem-1635	140	37	by	by	ADP
eurjchem-1635	140	38	tlc	tlc	NOUN
eurjchem-1635	140	39	and	and	CCONJ
eurjchem-1635	140	40	lc‐	lc‐	ADJ
eurjchem-1635	140	41	ms	ms	NOUN
eurjchem-1635	140	42	,	,	PUNCT
eurjchem-1635	140	43	after	after	ADP
eurjchem-1635	140	44	completion	completion	NOUN
eurjchem-1635	140	45	of	of	ADP
eurjchem-1635	140	46	reaction	reaction	NOUN
eurjchem-1635	140	47	,	,	PUNCT
eurjchem-1635	140	48	we	we	PRON
eurjchem-1635	140	49	evaporated	evaporate	VERB
eurjchem-1635	140	50	reaction	reaction	NOUN
eurjchem-1635	140	51	mass	mass	NOUN
eurjchem-1635	140	52	under	under	ADP
eurjchem-1635	140	53	reduced	reduced	ADJ
eurjchem-1635	140	54	pressure	pressure	NOUN
eurjchem-1635	140	55	to	to	PART
eurjchem-1635	140	56	obtain	obtain	VERB
eurjchem-1635	140	57	crude	crude	ADJ
eurjchem-1635	140	58	gummy	gummy	ADJ
eurjchem-1635	140	59	material	material	NOUN
eurjchem-1635	140	60	.	.	PUNCT
eurjchem-1635	141	1	the	the	DET
eurjchem-1635	141	2	reaction	reaction	NOUN
eurjchem-1635	141	3	mixture	mixture	NOUN
eurjchem-1635	141	4	was	be	AUX
eurjchem-1635	141	5	diluted	dilute	VERB
eurjchem-1635	141	6	with	with	ADP
eurjchem-1635	141	7	h2o	h2o	PROPN
eurjchem-1635	141	8	(	(	PUNCT
eurjchem-1635	141	9	10	10	NUM
eurjchem-1635	141	10	ml	ml	NOUN
eurjchem-1635	141	11	)	)	PUNCT
eurjchem-1635	141	12	and	and	CCONJ
eurjchem-1635	141	13	extracted	extract	VERB
eurjchem-1635	141	14	with	with	ADP
eurjchem-1635	141	15	dcm	dcm	PROPN
eurjchem-1635	141	16	(	(	PUNCT
eurjchem-1635	141	17	2	2	NUM
eurjchem-1635	141	18	×	×	NOUN
eurjchem-1635	141	19	10	10	NUM
eurjchem-1635	141	20	ml	ml	NOUN
eurjchem-1635	141	21	)	)	PUNCT
eurjchem-1635	141	22	.	.	PUNCT
eurjchem-1635	142	1	the	the	DET
eurjchem-1635	142	2	organic	organic	ADJ
eurjchem-1635	142	3	layer	layer	NOUN
eurjchem-1635	142	4	was	be	AUX
eurjchem-1635	142	5	washed	wash	VERB
eurjchem-1635	142	6	with	with	ADP
eurjchem-1635	142	7	sat	sit	VERB
eurjchem-1635	142	8	.	.	PUNCT
eurjchem-1635	143	1	nahco3	nahco3	ADJ
eurjchem-1635	143	2	solution	solution	NOUN
eurjchem-1635	143	3	(	(	PUNCT
eurjchem-1635	143	4	10	10	NUM
eurjchem-1635	143	5	ml	ml	NOUN
eurjchem-1635	143	6	)	)	PUNCT
eurjchem-1635	143	7	,	,	PUNCT
eurjchem-1635	143	8	and	and	CCONJ
eurjchem-1635	143	9	brine	brine	NOUN
eurjchem-1635	143	10	solution	solution	NOUN
eurjchem-1635	143	11	(	(	PUNCT
eurjchem-1635	143	12	10	10	NUM
eurjchem-1635	143	13	ml	ml	NOUN
eurjchem-1635	143	14	)	)	PUNCT
eurjchem-1635	143	15	,	,	PUNCT
eurjchem-1635	143	16	organic	organic	ADJ
eurjchem-1635	143	17	layer	layer	NOUN
eurjchem-1635	143	18	was	be	AUX
eurjchem-1635	143	19	dried	dry	VERB
eurjchem-1635	143	20	over	over	ADP
eurjchem-1635	143	21	anhydrous	anhydrous	ADJ
eurjchem-1635	143	22	na2so4	na2so4	NOUN
eurjchem-1635	143	23	and	and	CCONJ
eurjchem-1635	143	24	concentrated	concentrate	VERB
eurjchem-1635	143	25	in	in	ADP
eurjchem-1635	143	26	vacuum	vacuum	NOUN
eurjchem-1635	143	27	to	to	PART
eurjchem-1635	143	28	obtain	obtain	VERB
eurjchem-1635	143	29	2‐((benzylthio)methyl)‐3,4‐dihydro‐2h‐	2‐((benzylthio)methyl)‐3,4‐dihydro‐2h‐	NUM
eurjchem-1635	143	30	benzo[b][1,4]oxazine	benzo[b][1,4]oxazine	NOUN
eurjchem-1635	143	31	(	(	PUNCT
eurjchem-1635	143	32	6	6	NUM
eurjchem-1635	143	33	)	)	PUNCT
eurjchem-1635	143	34	.	.	PUNCT
eurjchem-1635	144	1	the	the	DET
eurjchem-1635	144	2	product	product	NOUN
eurjchem-1635	144	3	was	be	AUX
eurjchem-1635	144	4	confirmed	confirm	VERB
eurjchem-1635	144	5	by	by	ADP
eurjchem-1635	144	6	lc‐	lc‐	ADJ
eurjchem-1635	144	7	ms	ms	NOUN
eurjchem-1635	144	8	and	and	CCONJ
eurjchem-1635	144	9	used	use	VERB
eurjchem-1635	144	10	as	as	ADP
eurjchem-1635	144	11	such	such	ADJ
eurjchem-1635	144	12	for	for	ADP
eurjchem-1635	144	13	next	next	ADJ
eurjchem-1635	144	14	step	step	NOUN
eurjchem-1635	144	15	(	(	PUNCT
eurjchem-1635	144	16	scheme	scheme	NOUN
eurjchem-1635	144	17	2	2	NUM
eurjchem-1635	144	18	)	)	PUNCT
eurjchem-1635	144	19	.	.	PUNCT
eurjchem-1635	145	1	color	color	NOUN
eurjchem-1635	145	2	:	:	PUNCT
eurjchem-1635	145	3	yellow	yellow	ADJ
eurjchem-1635	145	4	.	.	PUNCT
eurjchem-1635	146	1	yield	yield	NOUN
eurjchem-1635	146	2	:	:	PUNCT
eurjchem-1635	146	3	85	85	NUM
eurjchem-1635	146	4	%	%	NOUN
eurjchem-1635	146	5	.	.	PUNCT
eurjchem-1635	147	1	ms	ms	NOUN
eurjchem-1635	147	2	(	(	PUNCT
eurjchem-1635	147	3	ei	ei	PROPN
eurjchem-1635	147	4	,	,	PUNCT
eurjchem-1635	147	5	m	m	PROPN
eurjchem-1635	147	6	/	/	SYM
eurjchem-1635	147	7	z	z	PROPN
eurjchem-1635	147	8	(	(	PUNCT
eurjchem-1635	147	9	%	%	NOUN
eurjchem-1635	147	10	)	)	PUNCT
eurjchem-1635	147	11	):	):	PUNCT
eurjchem-1635	147	12	272	272	NUM
eurjchem-1635	148	1	[	[	X
eurjchem-1635	148	2	m+h]+	m+h]+	X
eurjchem-1635	148	3	.	.	PROPN
eurjchem-1635	149	1	1h	1h	NUM
eurjchem-1635	149	2	nmr	nmr	NOUN
eurjchem-1635	149	3	(	(	PUNCT
eurjchem-1635	149	4	400	400	NUM
eurjchem-1635	149	5	mhz	mhz	NOUN
eurjchem-1635	149	6	,	,	PUNCT
eurjchem-1635	149	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	149	8	,	,	PUNCT
eurjchem-1635	149	9	δ	δ	PROPN
eurjchem-1635	149	10	,	,	PUNCT
eurjchem-1635	149	11	ppm	ppm	NOUN
eurjchem-1635	149	12	):	):	PUNCT
eurjchem-1635	149	13	7.38‐7.20	7.38‐7.20	NUM
eurjchem-1635	149	14	(	(	PUNCT
eurjchem-1635	149	15	m	m	PROPN
eurjchem-1635	149	16	,	,	PUNCT
eurjchem-1635	149	17	5h	5h	NUM
eurjchem-1635	149	18	,	,	PUNCT
eurjchem-1635	149	19	ar‐h	ar‐h	NOUN
eurjchem-1635	149	20	)	)	PUNCT
eurjchem-1635	149	21	,	,	PUNCT
eurjchem-1635	149	22	6.83‐6.78	6.83‐6.78	NUM
eurjchem-1635	149	23	(	(	PUNCT
eurjchem-1635	149	24	m	m	PROPN
eurjchem-1635	149	25	,	,	PUNCT
eurjchem-1635	149	26	2h	2h	NUM
eurjchem-1635	149	27	,	,	PUNCT
eurjchem-1635	149	28	ar‐h	ar‐h	NOUN
eurjchem-1635	149	29	)	)	PUNCT
eurjchem-1635	149	30	,	,	PUNCT
eurjchem-1635	149	31	6.61‐6.58	6.61‐6.58	NUM
eurjchem-1635	149	32	(	(	PUNCT
eurjchem-1635	149	33	m	m	PROPN
eurjchem-1635	149	34	,	,	PUNCT
eurjchem-1635	149	35	2h	2h	NUM
eurjchem-1635	149	36	,	,	PUNCT
eurjchem-1635	149	37	ar‐h	ar‐h	NOUN
eurjchem-1635	149	38	)	)	PUNCT
eurjchem-1635	149	39	,	,	PUNCT
eurjchem-1635	149	40	5.31	5.31	NUM
eurjchem-1635	149	41	(	(	PUNCT
eurjchem-1635	149	42	m	m	PROPN
eurjchem-1635	149	43	,	,	PUNCT
eurjchem-1635	149	44	1h	1h	NUM
eurjchem-1635	149	45	,	,	PUNCT
eurjchem-1635	149	46	ch2‐ch	ch2‐ch	NOUN
eurjchem-1635	149	47	)	)	PUNCT
eurjchem-1635	149	48	,	,	PUNCT
eurjchem-1635	149	49	4.01	4.01	NUM
eurjchem-1635	149	50	(	(	PUNCT
eurjchem-1635	149	51	br	br	PROPN
eurjchem-1635	149	52	,	,	PUNCT
eurjchem-1635	149	53	1h	1h	NUM
eurjchem-1635	149	54	,	,	PUNCT
eurjchem-1635	149	55	nh	nh	PROPN
eurjchem-1635	149	56	)	)	PUNCT
eurjchem-1635	149	57	,	,	PUNCT
eurjchem-1635	149	58	3.81‐3.60	3.81‐3.60	NUM
eurjchem-1635	149	59	(	(	PUNCT
eurjchem-1635	149	60	m	m	PROPN
eurjchem-1635	149	61	,	,	PUNCT
eurjchem-1635	149	62	4h	4h	NOUN
eurjchem-1635	149	63	,	,	PUNCT
eurjchem-1635	149	64	nh‐ch2	nh‐ch2	ADJ
eurjchem-1635	149	65	,	,	PUNCT
eurjchem-1635	149	66	ar‐ch2	ar‐ch2	NOUN
eurjchem-1635	149	67	)	)	PUNCT
eurjchem-1635	149	68	,	,	PUNCT
eurjchem-1635	149	69	2.94‐2.74	2.94‐2.74	NUM
eurjchem-1635	149	70	(	(	PUNCT
eurjchem-1635	149	71	m	m	PROPN
eurjchem-1635	149	72	,	,	PUNCT
eurjchem-1635	149	73	2h	2h	NUM
eurjchem-1635	149	74	,	,	PUNCT
eurjchem-1635	149	75	s‐ch2	s‐ch2	PROPN
eurjchem-1635	149	76	)	)	PUNCT
eurjchem-1635	149	77	.	.	PUNCT
eurjchem-1635	150	1	2.2.7	2.2.7	X
eurjchem-1635	150	2	.	.	PUNCT
eurjchem-1635	150	3	general	general	ADJ
eurjchem-1635	150	4	procedure	procedure	NOUN
eurjchem-1635	150	5	for	for	ADP
eurjchem-1635	150	6	the	the	DET
eurjchem-1635	150	7	synthesis	synthesis	NOUN
eurjchem-1635	150	8	of	of	ADP
eurjchem-1635	150	9	2‐((benzylthio	2‐((benzylthio	NOUN
eurjchem-1635	150	10	)	)	PUNCT
eurjchem-1635	150	11	methyl)‐3,4‐dihydro‐4‐substituted‐2h‐benzo[b][1,4]oxazine	methyl)‐3,4‐dihydro‐4‐substituted‐2h‐benzo[b][1,4]oxazine	NOUN
eurjchem-1635	150	12	(	(	PUNCT
eurjchem-1635	150	13	7a‐7e	7a‐7e	NUM
eurjchem-1635	150	14	)	)	PUNCT
eurjchem-1635	150	15	to	to	ADP
eurjchem-1635	150	16	a	a	DET
eurjchem-1635	150	17	stirred	stir	VERB
eurjchem-1635	150	18	solution	solution	NOUN
eurjchem-1635	150	19	of	of	ADP
eurjchem-1635	150	20	compound	compound	NOUN
eurjchem-1635	150	21	6	6	NUM
eurjchem-1635	150	22	(	(	PUNCT
eurjchem-1635	150	23	1	1	NUM
eurjchem-1635	150	24	equiv	equiv	NOUN
eurjchem-1635	150	25	.	.	PUNCT
eurjchem-1635	150	26	)	)	PUNCT
eurjchem-1635	151	1	in	in	ADP
eurjchem-1635	151	2	dcm	dcm	PROPN
eurjchem-1635	151	3	(	(	PUNCT
eurjchem-1635	151	4	10	10	NUM
eurjchem-1635	151	5	times	time	NOUN
eurjchem-1635	151	6	)	)	PUNCT
eurjchem-1635	151	7	was	be	AUX
eurjchem-1635	151	8	added	add	VERB
eurjchem-1635	151	9	pyridine	pyridine	NOUN
eurjchem-1635	151	10	(	(	PUNCT
eurjchem-1635	151	11	10	10	NUM
eurjchem-1635	151	12	times	time	NOUN
eurjchem-1635	151	13	)	)	PUNCT
eurjchem-1635	151	14	the	the	DET
eurjchem-1635	151	15	mixture	mixture	NOUN
eurjchem-1635	151	16	was	be	AUX
eurjchem-1635	151	17	stirred	stir	VERB
eurjchem-1635	151	18	at	at	ADP
eurjchem-1635	151	19	room	room	NOUN
eurjchem-1635	151	20	temperature	temperature	NOUN
eurjchem-1635	151	21	for	for	ADP
eurjchem-1635	151	22	15	15	NUM
eurjchem-1635	151	23	min	min	NOUN
eurjchem-1635	151	24	.	.	PROPN
eurjchem-1635	151	25	reaction	reaction	NOUN
eurjchem-1635	151	26	mixture	mixture	NOUN
eurjchem-1635	151	27	was	be	AUX
eurjchem-1635	151	28	cooled	cool	VERB
eurjchem-1635	151	29	to	to	ADP
eurjchem-1635	151	30	0	0	NUM
eurjchem-1635	151	31	°	°	ADP
eurjchem-1635	151	32	c	c	NOUN
eurjchem-1635	151	33	and	and	CCONJ
eurjchem-1635	151	34	substituted	substitute	VERB
eurjchem-1635	151	35	sulfonyl	sulfonyl	NOUN
eurjchem-1635	151	36	chloride	chloride	NOUN
eurjchem-1635	151	37	(	(	PUNCT
eurjchem-1635	151	38	1.2	1.2	NUM
eurjchem-1635	151	39	equiv	equiv	NOUN
eurjchem-1635	151	40	.	.	PUNCT
eurjchem-1635	151	41	)	)	PUNCT
eurjchem-1635	151	42	was	be	AUX
eurjchem-1635	151	43	added	add	VERB
eurjchem-1635	151	44	drop	drop	NOUN
eurjchem-1635	151	45	wise	wise	ADJ
eurjchem-1635	151	46	followed	follow	VERB
eurjchem-1635	151	47	by	by	ADP
eurjchem-1635	151	48	stirring	stir	VERB
eurjchem-1635	151	49	at	at	ADP
eurjchem-1635	151	50	room	room	NOUN
eurjchem-1635	151	51	temperature	temperature	NOUN
eurjchem-1635	151	52	for	for	ADP
eurjchem-1635	151	53	6	6	NUM
eurjchem-1635	151	54	h.	h.	NOUN
eurjchem-1635	151	55	the	the	DET
eurjchem-1635	151	56	reaction	reaction	NOUN
eurjchem-1635	151	57	was	be	AUX
eurjchem-1635	151	58	monitored	monitor	VERB
eurjchem-1635	151	59	by	by	ADP
eurjchem-1635	151	60	tlc	tlc	NOUN
eurjchem-1635	151	61	and	and	CCONJ
eurjchem-1635	151	62	lc‐ms	lc‐ms	NUM
eurjchem-1635	151	63	,	,	PUNCT
eurjchem-1635	151	64	after	after	SCONJ
eurjchem-1635	151	65	completion	completion	NOUN
eurjchem-1635	151	66	of	of	ADP
eurjchem-1635	151	67	reaction	reaction	NOUN
eurjchem-1635	151	68	mass	mass	NOUN
eurjchem-1635	151	69	was	be	AUX
eurjchem-1635	151	70	diluted	dilute	VERB
eurjchem-1635	151	71	with	with	ADP
eurjchem-1635	151	72	cold	cold	ADJ
eurjchem-1635	151	73	2	2	NUM
eurjchem-1635	151	74	n	n	NOUN
eurjchem-1635	151	75	hcl	hcl	NOUN
eurjchem-1635	151	76	and	and	CCONJ
eurjchem-1635	151	77	stirred	stir	VERB
eurjchem-1635	151	78	it	it	PRON
eurjchem-1635	151	79	for	for	ADP
eurjchem-1635	151	80	30	30	NUM
eurjchem-1635	151	81	min	min	NOUN
eurjchem-1635	151	82	.	.	PUNCT
eurjchem-1635	152	1	the	the	DET
eurjchem-1635	152	2	precipitation	precipitation	NOUN
eurjchem-1635	152	3	formed	form	VERB
eurjchem-1635	152	4	in	in	ADP
eurjchem-1635	152	5	reaction	reaction	NOUN
eurjchem-1635	152	6	mixture	mixture	NOUN
eurjchem-1635	152	7	.	.	PUNCT
eurjchem-1635	153	1	filtered	filter	VERB
eurjchem-1635	153	2	the	the	DET
eurjchem-1635	153	3	obtained	obtain	VERB
eurjchem-1635	153	4	solid	solid	ADJ
eurjchem-1635	153	5	and	and	CCONJ
eurjchem-1635	153	6	washed	wash	VERB
eurjchem-1635	153	7	it	it	PRON
eurjchem-1635	153	8	with	with	ADP
eurjchem-1635	153	9	excess	excess	NOUN
eurjchem-1635	153	10	of	of	ADP
eurjchem-1635	153	11	water	water	NOUN
eurjchem-1635	153	12	and	and	CCONJ
eurjchem-1635	153	13	cold	cold	ADJ
eurjchem-1635	153	14	diethyl	diethyl	NOUN
eurjchem-1635	153	15	ether	ether	NOUN
eurjchem-1635	153	16	and	and	CCONJ
eurjchem-1635	153	17	cold	cold	ADJ
eurjchem-1635	153	18	pentane	pentane	NOUN
eurjchem-1635	153	19	to	to	PART
eurjchem-1635	153	20	obtain	obtain	VERB
eurjchem-1635	153	21	all	all	DET
eurjchem-1635	153	22	compounds	compound	NOUN
eurjchem-1635	153	23	as	as	ADP
eurjchem-1635	153	24	white	white	ADJ
eurjchem-1635	153	25	solids	solid	NOUN
eurjchem-1635	153	26	.	.	PUNCT
eurjchem-1635	154	1	for	for	ADP
eurjchem-1635	154	2	filtrate	filtrate	NOUN
eurjchem-1635	154	3	extracted	extract	VERB
eurjchem-1635	154	4	with	with	ADP
eurjchem-1635	154	5	dcm	dcm	PROPN
eurjchem-1635	154	6	twice	twice	ADV
eurjchem-1635	154	7	.	.	PUNCT
eurjchem-1635	155	1	the	the	DET
eurjchem-1635	155	2	organic	organic	ADJ
eurjchem-1635	155	3	layer	layer	NOUN
eurjchem-1635	155	4	was	be	AUX
eurjchem-1635	155	5	washed	wash	VERB
eurjchem-1635	155	6	with	with	ADP
eurjchem-1635	155	7	brine	brine	NOUN
eurjchem-1635	155	8	solution	solution	NOUN
eurjchem-1635	155	9	;	;	PUNCT
eurjchem-1635	155	10	organic	organic	ADJ
eurjchem-1635	155	11	layer	layer	NOUN
eurjchem-1635	155	12	was	be	AUX
eurjchem-1635	155	13	evaporated	evaporate	VERB
eurjchem-1635	155	14	under	under	ADP
eurjchem-1635	155	15	reduced	reduce	VERB
eurjchem-1635	155	16	pressure	pressure	NOUN
eurjchem-1635	155	17	to	to	PART
eurjchem-1635	155	18	get	get	AUX
eurjchem-1635	155	19	desired	desire	VERB
eurjchem-1635	155	20	2‐((benzylthio)methyl)‐3,4‐dihydro‐4‐substituted‐2h‐	2‐((benzylthio)methyl)‐3,4‐dihydro‐4‐substituted‐2h‐	NUM
eurjchem-1635	155	21	benzo[b][1,4]oxazine	benzo[b][1,4]oxazine	NOUN
eurjchem-1635	155	22	derivatives	derivative	NOUN
eurjchem-1635	155	23	(	(	PUNCT
eurjchem-1635	155	24	7a‐e	7a‐e	PROPN
eurjchem-1635	155	25	)	)	PUNCT
eurjchem-1635	155	26	(	(	PUNCT
eurjchem-1635	155	27	scheme	scheme	NOUN
eurjchem-1635	155	28	2	2	NUM
eurjchem-1635	155	29	)	)	PUNCT
eurjchem-1635	155	30	.	.	PUNCT
eurjchem-1635	156	1	2‐((benzylthio)methyl)‐4‐(phenylsulfonyl)‐3,4‐dihydro‐2h‐	2‐((benzylthio)methyl)‐4‐(phenylsulfonyl)‐3,4‐dihydro‐2h‐	NUM
eurjchem-1635	156	2	benzo[b][1,4]oxazine	benzo[b][1,4]oxazine	NOUN
eurjchem-1635	156	3	(	(	PUNCT
eurjchem-1635	156	4	7a	7a	NUM
eurjchem-1635	156	5	):	):	PUNCT
eurjchem-1635	156	6	color	color	NOUN
eurjchem-1635	156	7	:	:	PUNCT
eurjchem-1635	156	8	white	white	ADJ
eurjchem-1635	156	9	.	.	PUNCT
eurjchem-1635	157	1	yield	yield	NOUN
eurjchem-1635	157	2	:	:	PUNCT
eurjchem-1635	157	3	95	95	NUM
eurjchem-1635	157	4	%	%	NOUN
eurjchem-1635	157	5	.	.	PUNCT
eurjchem-1635	158	1	m.p	m.p	PROPN
eurjchem-1635	158	2	.	.	PROPN
eurjchem-1635	158	3	:	:	PUNCT
eurjchem-1635	159	1	164‐	164‐	NUM
eurjchem-1635	159	2	165	165	NUM
eurjchem-1635	159	3	°	°	PROPN
eurjchem-1635	159	4	c	c	NOUN
eurjchem-1635	159	5	.	.	PUNCT
eurjchem-1635	160	1	1h	1h	NUM
eurjchem-1635	160	2	nmr	nmr	NOUN
eurjchem-1635	160	3	(	(	PUNCT
eurjchem-1635	160	4	400	400	NUM
eurjchem-1635	160	5	mhz	mhz	NOUN
eurjchem-1635	160	6	,	,	PUNCT
eurjchem-1635	160	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	160	8	,	,	PUNCT
eurjchem-1635	160	9	δ	δ	PROPN
eurjchem-1635	160	10	,	,	PUNCT
eurjchem-1635	160	11	ppm	ppm	NUM
eurjchem-1635	160	12	):	):	PUNCT
eurjchem-1635	160	13	7.90	7.90	NUM
eurjchem-1635	160	14	(	(	PUNCT
eurjchem-1635	160	15	d	d	PROPN
eurjchem-1635	160	16	,	,	PUNCT
eurjchem-1635	160	17	2h	2h	NUM
eurjchem-1635	160	18	,	,	PUNCT
eurjchem-1635	160	19	j	j	PROPN
eurjchem-1635	160	20	=	=	SYM
eurjchem-1635	160	21	7.6	7.6	NUM
eurjchem-1635	160	22	hz	hz	NOUN
eurjchem-1635	160	23	,	,	PUNCT
eurjchem-1635	160	24	ar‐h	ar‐h	NOUN
eurjchem-1635	160	25	)	)	PUNCT
eurjchem-1635	160	26	,	,	PUNCT
eurjchem-1635	160	27	7.64‐7.58	7.64‐7.58	NUM
eurjchem-1635	160	28	(	(	PUNCT
eurjchem-1635	160	29	d	d	PROPN
eurjchem-1635	160	30	,	,	PUNCT
eurjchem-1635	160	31	1h	1h	NUM
eurjchem-1635	160	32	,	,	PUNCT
eurjchem-1635	160	33	j	j	PROPN
eurjchem-1635	160	34	=	=	SYM
eurjchem-1635	160	35	7.2	7.2	NUM
eurjchem-1635	160	36	hz	hz	NOUN
eurjchem-1635	160	37	,	,	PUNCT
eurjchem-1635	160	38	ar‐h	ar‐h	NOUN
eurjchem-1635	160	39	)	)	PUNCT
eurjchem-1635	160	40	,	,	PUNCT
eurjchem-1635	160	41	7.56‐7.55	7.56‐7.55	PROPN
eurjchem-1635	160	42	(	(	PUNCT
eurjchem-1635	160	43	m	m	PROPN
eurjchem-1635	160	44	,	,	PUNCT
eurjchem-1635	160	45	2h	2h	NUM
eurjchem-1635	160	46	,	,	PUNCT
eurjchem-1635	160	47	ar‐h	ar‐h	NOUN
eurjchem-1635	160	48	)	)	PUNCT
eurjchem-1635	160	49	,	,	PUNCT
eurjchem-1635	160	50	7.31‐7.27	7.31‐7.27	NUM
eurjchem-1635	160	51	(	(	PUNCT
eurjchem-1635	160	52	m	m	PROPN
eurjchem-1635	160	53	,	,	PUNCT
eurjchem-1635	160	54	2h	2h	NUM
eurjchem-1635	160	55	,	,	PUNCT
eurjchem-1635	160	56	j	j	PROPN
eurjchem-1635	160	57	=	=	SYM
eurjchem-1635	160	58	6.8	6.8	NUM
eurjchem-1635	160	59	hz	hz	NOUN
eurjchem-1635	160	60	,	,	PUNCT
eurjchem-1635	160	61	ar‐h	ar‐h	NOUN
eurjchem-1635	160	62	)	)	PUNCT
eurjchem-1635	160	63	,	,	PUNCT
eurjchem-1635	160	64	7.24‐7.20	7.24‐7.20	NUM
eurjchem-1635	160	65	(	(	PUNCT
eurjchem-1635	160	66	m	m	PROPN
eurjchem-1635	160	67	,	,	PUNCT
eurjchem-1635	160	68	3h	3h	NUM
eurjchem-1635	160	69	,	,	PUNCT
eurjchem-1635	160	70	ar‐h	ar‐h	NOUN
eurjchem-1635	160	71	)	)	PUNCT
eurjchem-1635	160	72	,	,	PUNCT
eurjchem-1635	160	73	6.68‐6.60	6.68‐6.60	NUM
eurjchem-1635	160	74	(	(	PUNCT
eurjchem-1635	160	75	m	m	PROPN
eurjchem-1635	160	76	,	,	PUNCT
eurjchem-1635	160	77	2h	2h	NUM
eurjchem-1635	160	78	,	,	PUNCT
eurjchem-1635	160	79	ar‐h	ar‐h	NOUN
eurjchem-1635	160	80	)	)	PUNCT
eurjchem-1635	160	81	,	,	PUNCT
eurjchem-1635	160	82	6.62	6.62	NUM
eurjchem-1635	160	83	(	(	PUNCT
eurjchem-1635	160	84	t	t	PROPN
eurjchem-1635	160	85	,	,	PUNCT
eurjchem-1635	160	86	1h	1h	NUM
eurjchem-1635	160	87	,	,	PUNCT
eurjchem-1635	160	88	j	j	PROPN
eurjchem-1635	160	89	=	=	SYM
eurjchem-1635	160	90	8.0	8.0	NUM
eurjchem-1635	160	91	hz	hz	NOUN
eurjchem-1635	160	92	,	,	PUNCT
eurjchem-1635	160	93	ar‐h	ar‐h	PROPN
eurjchem-1635	160	94	)	)	PUNCT
eurjchem-1635	160	95	,	,	PUNCT
eurjchem-1635	160	96	6.51	6.51	NUM
eurjchem-1635	160	97	(	(	PUNCT
eurjchem-1635	160	98	t	t	PROPN
eurjchem-1635	160	99	,	,	PUNCT
eurjchem-1635	160	100	1h	1h	NUM
eurjchem-1635	160	101	,	,	PUNCT
eurjchem-1635	160	102	j	j	PROPN
eurjchem-1635	160	103	=	=	SYM
eurjchem-1635	160	104	7.2	7.2	NUM
eurjchem-1635	160	105	hz	hz	NOUN
eurjchem-1635	160	106	,	,	PUNCT
eurjchem-1635	160	107	ar‐h	ar‐h	PROPN
eurjchem-1635	160	108	)	)	PUNCT
eurjchem-1635	160	109	,	,	PUNCT
eurjchem-1635	160	110	4.12	4.12	NUM
eurjchem-1635	160	111	(	(	PUNCT
eurjchem-1635	160	112	m	m	PROPN
eurjchem-1635	160	113	,	,	PUNCT
eurjchem-1635	160	114	2h	2h	NUM
eurjchem-1635	160	115	,	,	PUNCT
eurjchem-1635	160	116	ch2‐ch	ch2‐ch	PRON
eurjchem-1635	160	117	,	,	PUNCT
eurjchem-1635	160	118	s‐ch2	s‐ch2	PROPN
eurjchem-1635	160	119	)	)	PUNCT
eurjchem-1635	160	120	,	,	PUNCT
eurjchem-1635	160	121	4.08	4.08	NUM
eurjchem-1635	160	122	(	(	PUNCT
eurjchem-1635	160	123	q	q	NOUN
eurjchem-1635	160	124	,	,	PUNCT
eurjchem-1635	160	125	1h	1h	NUM
eurjchem-1635	160	126	,	,	PUNCT
eurjchem-1635	160	127	s‐ch2	s‐ch2	PROPN
eurjchem-1635	160	128	)	)	PUNCT
eurjchem-1635	160	129	,	,	PUNCT
eurjchem-1635	160	130	3.32‐3.29	3.32‐3.29	NUM
eurjchem-1635	160	131	(	(	PUNCT
eurjchem-1635	160	132	dd	dd	PROPN
eurjchem-1635	160	133	,	,	PUNCT
eurjchem-1635	160	134	1h	1h	NUM
eurjchem-1635	160	135	,	,	PUNCT
eurjchem-1635	160	136	n‐ch2	n‐ch2	PROPN
eurjchem-1635	160	137	)	)	PUNCT
eurjchem-1635	160	138	,	,	PUNCT
eurjchem-1635	160	139	3.12‐3.09	3.12‐3.09	NUM
eurjchem-1635	160	140	(	(	PUNCT
eurjchem-1635	160	141	m	m	PROPN
eurjchem-1635	160	142	,	,	PUNCT
eurjchem-1635	160	143	1h	1h	NUM
eurjchem-1635	160	144	,	,	PUNCT
eurjchem-1635	160	145	n‐	n‐	NOUN
eurjchem-1635	160	146	ch2	ch2	PROPN
eurjchem-1635	160	147	)	)	PUNCT
eurjchem-1635	160	148	,	,	PUNCT
eurjchem-1635	160	149	2.99	2.99	NUM
eurjchem-1635	160	150	(	(	PUNCT
eurjchem-1635	160	151	d	d	NOUN
eurjchem-1635	160	152	,	,	PUNCT
eurjchem-1635	160	153	2h	2h	NUM
eurjchem-1635	160	154	,	,	PUNCT
eurjchem-1635	160	155	j=	j=	ADV
eurjchem-1635	160	156	6	6	NUM
eurjchem-1635	160	157	hz	hz	VERB
eurjchem-1635	160	158	,	,	PUNCT
eurjchem-1635	160	159	ch‐ch2	ch‐ch2	PROPN
eurjchem-1635	160	160	)	)	PUNCT
eurjchem-1635	160	161	.	.	PUNCT
eurjchem-1635	161	1	13c	13c	NOUN
eurjchem-1635	161	2	nmr	nmr	NOUN
eurjchem-1635	161	3	(	(	PUNCT
eurjchem-1635	161	4	100	100	NUM
eurjchem-1635	161	5	mhz	mhz	NOUN
eurjchem-1635	161	6	,	,	PUNCT
eurjchem-1635	161	7	cdcl3	cdcl3	PROPN
eurjchem-1635	161	8	,	,	PUNCT
eurjchem-1635	161	9	δ	δ	PROPN
eurjchem-1635	161	10	,	,	PUNCT
eurjchem-1635	161	11	ppm	ppm	NOUN
eurjchem-1635	161	12	):	):	PUNCT
eurjchem-1635	161	13	141.12	141.12	NUM
eurjchem-1635	161	14	,	,	PUNCT
eurjchem-1635	161	15	140.11	140.11	NUM
eurjchem-1635	161	16	,	,	PUNCT
eurjchem-1635	161	17	139.38	139.38	NUM
eurjchem-1635	161	18	,	,	PUNCT
eurjchem-1635	161	19	135.36	135.36	NUM
eurjchem-1635	161	20	,	,	PUNCT
eurjchem-1635	161	21	129.2	129.2	NUM
eurjchem-1635	161	22	,	,	PUNCT
eurjchem-1635	161	23	128.78	128.78	NUM
eurjchem-1635	161	24	,	,	PUNCT
eurjchem-1635	161	25	128.12	128.12	NUM
eurjchem-1635	161	26	,	,	PUNCT
eurjchem-1635	161	27	127.66	127.66	NUM
eurjchem-1635	161	28	,	,	PUNCT
eurjchem-1635	161	29	127.11	127.11	NUM
eurjchem-1635	161	30	,	,	PUNCT
eurjchem-1635	161	31	127.10	127.10	NUM
eurjchem-1635	161	32	,	,	PUNCT
eurjchem-1635	161	33	127.01	127.01	NUM
eurjchem-1635	161	34	,	,	PUNCT
eurjchem-1635	161	35	126.12	126.12	NUM
eurjchem-1635	161	36	,	,	PUNCT
eurjchem-1635	161	37	125.11	125.11	NUM
eurjchem-1635	161	38	,	,	PUNCT
eurjchem-1635	161	39	125.10	125.10	NUM
eurjchem-1635	161	40	,	,	PUNCT
eurjchem-1635	161	41	115.12	115.12	NUM
eurjchem-1635	161	42	,	,	PUNCT
eurjchem-1635	161	43	115.10	115.10	NUM
eurjchem-1635	161	44	,	,	PUNCT
eurjchem-1635	161	45	110.22	110.22	NUM
eurjchem-1635	161	46	,	,	PUNCT
eurjchem-1635	161	47	110.14	110.14	NUM
eurjchem-1635	161	48	,	,	PUNCT
eurjchem-1635	161	49	78.30	78.30	NUM
eurjchem-1635	161	50	,	,	PUNCT
eurjchem-1635	161	51	54.12	54.12	NUM
eurjchem-1635	161	52	,	,	PUNCT
eurjchem-1635	161	53	38.15	38.15	NUM
eurjchem-1635	161	54	,	,	PUNCT
eurjchem-1635	161	55	38.10	38.10	NUM
eurjchem-1635	161	56	.	.	PUNCT
eurjchem-1635	162	1	ms	ms	NOUN
eurjchem-1635	162	2	(	(	PUNCT
eurjchem-1635	162	3	ei	ei	PROPN
eurjchem-1635	162	4	,	,	PUNCT
eurjchem-1635	162	5	m	m	PROPN
eurjchem-1635	162	6	/	/	SYM
eurjchem-1635	162	7	z	z	PROPN
eurjchem-1635	162	8	(	(	PUNCT
eurjchem-1635	162	9	%	%	NOUN
eurjchem-1635	162	10	)	)	PUNCT
eurjchem-1635	162	11	):	):	PUNCT
eurjchem-1635	162	12	412	412	NUM
eurjchem-1635	163	1	[	[	X
eurjchem-1635	163	2	m+h	m+h	NOUN
eurjchem-1635	163	3	]	]	PUNCT
eurjchem-1635	163	4	.	.	PUNCT
eurjchem-1635	164	1	hplc	hplc	NOUN
eurjchem-1635	164	2	:	:	PUNCT
eurjchem-1635	164	3	purity	purity	NOUN
eurjchem-1635	164	4	=	=	SYM
eurjchem-1635	165	1	98.0	98.0	NUM
eurjchem-1635	165	2	%	%	NOUN
eurjchem-1635	165	3	,	,	PUNCT
eurjchem-1635	165	4	r.t	r.t	PROPN
eurjchem-1635	165	5	.	.	PUNCT
eurjchem-1635	166	1	=	=	PROPN
eurjchem-1635	166	2	8.12	8.12	NUM
eurjchem-1635	166	3	min	min	NOUN
eurjchem-1635	166	4	.	.	PROPN
eurjchem-1635	166	5	2‐((benzylthio)methyl)‐4‐tosyl‐3	2‐((benzylthio)methyl)‐4‐tosyl‐3	NUM
eurjchem-1635	166	6	,	,	PUNCT
eurjchem-1635	166	7	4‐dihydro‐2h‐benzo[b	4‐dihydro‐2h‐benzo[b	NUM
eurjchem-1635	166	8	]	]	PUNCT
eurjchem-1635	167	1	[	[	X
eurjchem-1635	167	2	1	1	NUM
eurjchem-1635	167	3	,	,	PUNCT
eurjchem-1635	167	4	4]oxazine	4]oxazine	PROPN
eurjchem-1635	167	5	(	(	PUNCT
eurjchem-1635	167	6	7b	7b	NUM
eurjchem-1635	167	7	):	):	PUNCT
eurjchem-1635	167	8	color	color	NOUN
eurjchem-1635	167	9	:	:	PUNCT
eurjchem-1635	167	10	white	white	ADJ
eurjchem-1635	167	11	.	.	PUNCT
eurjchem-1635	168	1	yield	yield	NOUN
eurjchem-1635	168	2	:	:	PUNCT
eurjchem-1635	168	3	94	94	NUM
eurjchem-1635	168	4	%	%	NOUN
eurjchem-1635	168	5	.	.	PUNCT
eurjchem-1635	169	1	m.p	m.p	PROPN
eurjchem-1635	169	2	.	.	PROPN
eurjchem-1635	169	3	:	:	PUNCT
eurjchem-1635	170	1	169‐170	169‐170	NUM
eurjchem-1635	170	2	°	°	SYM
eurjchem-1635	170	3	c	c	PROPN
eurjchem-1635	170	4	.	.	PUNCT
eurjchem-1635	171	1	1h	1h	NUM
eurjchem-1635	171	2	nmr	nmr	NOUN
eurjchem-1635	171	3	(	(	PUNCT
eurjchem-1635	171	4	400	400	NUM
eurjchem-1635	171	5	mhz	mhz	NOUN
eurjchem-1635	171	6	,	,	PUNCT
eurjchem-1635	171	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	171	8	,	,	PUNCT
eurjchem-1635	171	9	δ	δ	PROPN
eurjchem-1635	171	10	,	,	PUNCT
eurjchem-1635	171	11	ppm	ppm	NOUN
eurjchem-1635	171	12	):	):	PUNCT
eurjchem-1635	171	13	7.72‐7.68	7.72‐7.68	PROPN
eurjchem-1635	171	14	(	(	PUNCT
eurjchem-1635	171	15	d	d	PROPN
eurjchem-1635	171	16	,	,	PUNCT
eurjchem-1635	171	17	4h	4h	NUM
eurjchem-1635	171	18	,	,	PUNCT
eurjchem-1635	171	19	ar‐h	ar‐h	PROPN
eurjchem-1635	171	20	)	)	PUNCT
eurjchem-1635	171	21	,	,	PUNCT
eurjchem-1635	171	22	7.39‐7.37	7.39‐7.37	PROPN
eurjchem-1635	171	23	(	(	PUNCT
eurjchem-1635	171	24	d	d	PROPN
eurjchem-1635	171	25	,	,	PUNCT
eurjchem-1635	171	26	2h	2h	NUM
eurjchem-1635	171	27	,	,	PUNCT
eurjchem-1635	171	28	j	j	PROPN
eurjchem-1635	171	29	=	=	PROPN
eurjchem-1635	171	30	8.4	8.4	NUM
eurjchem-1635	171	31	hz	hz	NOUN
eurjchem-1635	171	32	,	,	PUNCT
eurjchem-1635	171	33	ar‐h	ar‐h	PROPN
eurjchem-1635	171	34	)	)	PUNCT
eurjchem-1635	171	35	,	,	PUNCT
eurjchem-1635	171	36	7.34‐7.30	7.34‐7.30	NUM
eurjchem-1635	171	37	(	(	PUNCT
eurjchem-1635	171	38	m	m	PROPN
eurjchem-1635	171	39	,	,	PUNCT
eurjchem-1635	171	40	2h	2h	NUM
eurjchem-1635	171	41	,	,	PUNCT
eurjchem-1635	171	42	ar‐h	ar‐h	NOUN
eurjchem-1635	171	43	)	)	PUNCT
eurjchem-1635	171	44	,	,	PUNCT
eurjchem-1635	171	45	7.26‐7.24	7.26‐7.24	NUM
eurjchem-1635	171	46	(	(	PUNCT
eurjchem-1635	171	47	m	m	PROPN
eurjchem-1635	171	48	,	,	PUNCT
eurjchem-1635	171	49	1h	1h	NUM
eurjchem-1635	171	50	,	,	PUNCT
eurjchem-1635	171	51	ar‐h	ar‐h	NOUN
eurjchem-1635	171	52	)	)	PUNCT
eurjchem-1635	171	53	,	,	PUNCT
eurjchem-1635	171	54	6.88‐6.63	6.88‐6.63	PROPN
eurjchem-1635	171	55	(	(	PUNCT
eurjchem-1635	171	56	m	m	PROPN
eurjchem-1635	171	57	,	,	PUNCT
eurjchem-1635	171	58	3h	3h	NUM
eurjchem-1635	171	59	,	,	PUNCT
eurjchem-1635	171	60	ar‐h	ar‐h	NOUN
eurjchem-1635	171	61	)	)	PUNCT
eurjchem-1635	171	62	,	,	PUNCT
eurjchem-1635	171	63	6.51	6.51	NUM
eurjchem-1635	171	64	(	(	PUNCT
eurjchem-1635	171	65	t	t	PROPN
eurjchem-1635	171	66	,	,	PUNCT
eurjchem-1635	171	67	1h	1h	NUM
eurjchem-1635	171	68	,	,	PUNCT
eurjchem-1635	171	69	j	j	PROPN
eurjchem-1635	171	70	=	=	SYM
eurjchem-1635	171	71	6.2	6.2	NUM
eurjchem-1635	171	72	hz	hz	NOUN
eurjchem-1635	171	73	,	,	PUNCT
eurjchem-1635	171	74	ar‐h	ar‐h	PROPN
eurjchem-1635	171	75	)	)	PUNCT
eurjchem-1635	171	76	,	,	PUNCT
eurjchem-1635	171	77	4.12	4.12	NUM
eurjchem-1635	171	78	(	(	PUNCT
eurjchem-1635	171	79	m	m	PROPN
eurjchem-1635	171	80	,	,	PUNCT
eurjchem-1635	171	81	2h	2h	NUM
eurjchem-1635	171	82	,	,	PUNCT
eurjchem-1635	171	83	ch2‐ch	ch2‐ch	PRON
eurjchem-1635	171	84	,	,	PUNCT
eurjchem-1635	171	85	s‐ch2	s‐ch2	PROPN
eurjchem-1635	171	86	)	)	PUNCT
eurjchem-1635	171	87	,	,	PUNCT
eurjchem-1635	171	88	4.06	4.06	NUM
eurjchem-1635	171	89	(	(	PUNCT
eurjchem-1635	171	90	q	q	NOUN
eurjchem-1635	171	91	,	,	PUNCT
eurjchem-1635	171	92	1h	1h	NUM
eurjchem-1635	171	93	,	,	PUNCT
eurjchem-1635	171	94	s‐	s‐	PROPN
eurjchem-1635	171	95	ch2	ch2	PROPN
eurjchem-1635	171	96	)	)	PUNCT
eurjchem-1635	171	97	,	,	PUNCT
eurjchem-1635	171	98	3.36‐3.32	3.36‐3.32	NUM
eurjchem-1635	171	99	(	(	PUNCT
eurjchem-1635	171	100	dd	dd	PROPN
eurjchem-1635	171	101	,	,	PUNCT
eurjchem-1635	171	102	1h	1h	NUM
eurjchem-1635	171	103	,	,	PUNCT
eurjchem-1635	171	104	n‐ch2	n‐ch2	PROPN
eurjchem-1635	171	105	)	)	PUNCT
eurjchem-1635	171	106	,	,	PUNCT
eurjchem-1635	171	107	3.18‐3.08	3.18‐3.08	NUM
eurjchem-1635	171	108	(	(	PUNCT
eurjchem-1635	171	109	m	m	PROPN
eurjchem-1635	171	110	,	,	PUNCT
eurjchem-1635	171	111	1h	1h	NUM
eurjchem-1635	171	112	,	,	PUNCT
eurjchem-1635	171	113	n‐ch2	n‐ch2	PROPN
eurjchem-1635	171	114	)	)	PUNCT
eurjchem-1635	171	115	,	,	PUNCT
eurjchem-1635	171	116	2.98	2.98	NUM
eurjchem-1635	171	117	(	(	PUNCT
eurjchem-1635	171	118	d	d	NOUN
eurjchem-1635	171	119	,	,	PUNCT
eurjchem-1635	171	120	j=6	j=6	PROPN
eurjchem-1635	171	121	hz	hz	NOUN
eurjchem-1635	171	122	,	,	PUNCT
eurjchem-1635	171	123	2h	2h	NUM
eurjchem-1635	171	124	,	,	PUNCT
eurjchem-1635	171	125	ch‐ch2	ch‐ch2	PROPN
eurjchem-1635	171	126	)	)	PUNCT
eurjchem-1635	171	127	,	,	PUNCT
eurjchem-1635	171	128	2.37	2.37	NUM
eurjchem-1635	171	129	(	(	PUNCT
eurjchem-1635	171	130	s	s	PROPN
eurjchem-1635	171	131	,	,	PUNCT
eurjchem-1635	171	132	3h	3h	NUM
eurjchem-1635	171	133	,	,	PUNCT
eurjchem-1635	171	134	ar‐ch3	ar‐ch3	PROPN
eurjchem-1635	171	135	)	)	PUNCT
eurjchem-1635	171	136	.	.	PUNCT
eurjchem-1635	172	1	13c	13c	NOUN
eurjchem-1635	172	2	nmr	nmr	NOUN
eurjchem-1635	172	3	(	(	PUNCT
eurjchem-1635	172	4	100	100	NUM
eurjchem-1635	172	5	mhz	mhz	NOUN
eurjchem-1635	172	6	,	,	PUNCT
eurjchem-1635	172	7	cdcl3	cdcl3	PROPN
eurjchem-1635	172	8	,	,	PUNCT
eurjchem-1635	172	9	δ	δ	PROPN
eurjchem-1635	172	10	,	,	PUNCT
eurjchem-1635	172	11	ppm	ppm	NUM
eurjchem-1635	172	12	):	):	PUNCT
eurjchem-1635	172	13	141.22	141.22	NUM
eurjchem-1635	172	14	,	,	PUNCT
eurjchem-1635	172	15	140.11	140.11	NUM
eurjchem-1635	172	16	,	,	PUNCT
eurjchem-1635	172	17	139.48	139.48	NUM
eurjchem-1635	172	18	,	,	PUNCT
eurjchem-1635	172	19	135.36	135.36	NUM
eurjchem-1635	172	20	,	,	PUNCT
eurjchem-1635	172	21	129.22	129.22	NUM
eurjchem-1635	172	22	,	,	PUNCT
eurjchem-1635	172	23	128.22	128.22	NUM
eurjchem-1635	172	24	,	,	PUNCT
eurjchem-1635	172	25	127.66	127.66	NUM
eurjchem-1635	172	26	,	,	PUNCT
eurjchem-1635	172	27	127.11	127.11	NUM
eurjchem-1635	172	28	,	,	PUNCT
eurjchem-1635	172	29	127.10	127.10	NUM
eurjchem-1635	172	30	,	,	PUNCT
eurjchem-1635	172	31	127.01	127.01	NUM
eurjchem-1635	172	32	,	,	PUNCT
eurjchem-1635	172	33	126.12	126.12	NUM
eurjchem-1635	172	34	,	,	PUNCT
eurjchem-1635	172	35	125.11	125.11	NUM
eurjchem-1635	172	36	,	,	PUNCT
eurjchem-1635	172	37	125.1	125.1	NUM
eurjchem-1635	172	38	,	,	PUNCT
eurjchem-1635	172	39	115.12	115.12	NUM
eurjchem-1635	172	40	,	,	PUNCT
eurjchem-1635	172	41	115.10	115.10	NUM
eurjchem-1635	172	42	,	,	PUNCT
eurjchem-1635	172	43	110.22	110.22	NUM
eurjchem-1635	172	44	,	,	PUNCT
eurjchem-1635	172	45	110.14	110.14	NUM
eurjchem-1635	172	46	,	,	PUNCT
eurjchem-1635	172	47	78.31	78.31	NUM
eurjchem-1635	172	48	,	,	PUNCT
eurjchem-1635	172	49	54.12	54.12	NUM
eurjchem-1635	172	50	,	,	PUNCT
eurjchem-1635	172	51	38.14	38.14	NUM
eurjchem-1635	172	52	,	,	PUNCT
eurjchem-1635	172	53	38.11	38.11	NUM
eurjchem-1635	172	54	,	,	PUNCT
eurjchem-1635	172	55	23.64	23.64	NUM
eurjchem-1635	172	56	.	.	PUNCT
eurjchem-1635	173	1	ms	ms	NOUN
eurjchem-1635	173	2	(	(	PUNCT
eurjchem-1635	173	3	ei	ei	PROPN
eurjchem-1635	173	4	,	,	PUNCT
eurjchem-1635	173	5	m	m	PROPN
eurjchem-1635	173	6	/	/	SYM
eurjchem-1635	173	7	z	z	PROPN
eurjchem-1635	173	8	(	(	PUNCT
eurjchem-1635	173	9	%	%	NOUN
eurjchem-1635	173	10	)	)	PUNCT
eurjchem-1635	173	11	):	):	PUNCT
eurjchem-1635	173	12	426	426	NUM
eurjchem-1635	174	1	[	[	X
eurjchem-1635	174	2	m+h	m+h	NOUN
eurjchem-1635	174	3	]	]	X
eurjchem-1635	174	4	.	.	PUNCT
eurjchem-1635	175	1	hplc	hplc	NOUN
eurjchem-1635	175	2	:	:	PUNCT
eurjchem-1635	175	3	purity	purity	NOUN
eurjchem-1635	175	4	=	=	NOUN
eurjchem-1635	175	5	98.4	98.4	NUM
eurjchem-1635	175	6	%	%	NOUN
eurjchem-1635	175	7	,	,	PUNCT
eurjchem-1635	175	8	r.t	r.t	PROPN
eurjchem-1635	175	9	.	.	PUNCT
eurjchem-1635	175	10	=	=	NUM
eurjchem-1635	175	11	7.17	7.17	NUM
eurjchem-1635	175	12	min	min	NOUN
eurjchem-1635	175	13	.	.	PROPN
eurjchem-1635	175	14	2‐((benzylthio)methyl)‐4‐((4‐chlorophenyl)sulfonyl)‐3	2‐((benzylthio)methyl)‐4‐((4‐chlorophenyl)sulfonyl)‐3	NUM
eurjchem-1635	175	15	,	,	PUNCT
eurjchem-1635	175	16	4‐di	4‐di	NUM
eurjchem-1635	175	17	hydro‐2h‐benzo[b][1,4]oxazine	hydro‐2h‐benzo[b][1,4]oxazine	NUM
eurjchem-1635	175	18	(	(	PUNCT
eurjchem-1635	175	19	7c	7c	NOUN
eurjchem-1635	175	20	):	):	PUNCT
eurjchem-1635	175	21	color	color	NOUN
eurjchem-1635	175	22	:	:	PUNCT
eurjchem-1635	175	23	white	white	ADJ
eurjchem-1635	175	24	.	.	PUNCT
eurjchem-1635	176	1	yield	yield	NOUN
eurjchem-1635	176	2	:	:	PUNCT
eurjchem-1635	176	3	87	87	NUM
eurjchem-1635	176	4	%	%	NOUN
eurjchem-1635	176	5	.	.	PUNCT
eurjchem-1635	177	1	m.p	m.p	PROPN
eurjchem-1635	177	2	.	.	PROPN
eurjchem-1635	177	3	:	:	PUNCT
eurjchem-1635	178	1	181‐182	181‐182	NUM
eurjchem-1635	178	2	°	°	NUM
eurjchem-1635	178	3	c	c	PROPN
eurjchem-1635	178	4	.	.	PUNCT
eurjchem-1635	179	1	1h	1h	NUM
eurjchem-1635	179	2	nmr	nmr	NOUN
eurjchem-1635	179	3	(	(	PUNCT
eurjchem-1635	179	4	400	400	NUM
eurjchem-1635	179	5	mhz	mhz	NOUN
eurjchem-1635	179	6	,	,	PUNCT
eurjchem-1635	179	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	179	8	,	,	PUNCT
eurjchem-1635	179	9	δ	δ	PROPN
eurjchem-1635	179	10	,	,	PUNCT
eurjchem-1635	179	11	ppm	ppm	NOUN
eurjchem-1635	179	12	):	):	PUNCT
eurjchem-1635	179	13	7.79‐	7.79‐	NUM
eurjchem-1635	179	14	7.71	7.71	NUM
eurjchem-1635	179	15	(	(	PUNCT
eurjchem-1635	179	16	d	d	NOUN
eurjchem-1635	179	17	,	,	PUNCT
eurjchem-1635	179	18	2h	2h	NUM
eurjchem-1635	179	19	,	,	PUNCT
eurjchem-1635	179	20	j	j	PROPN
eurjchem-1635	179	21	=	=	PROPN
eurjchem-1635	179	22	8.4	8.4	NUM
eurjchem-1635	179	23	hz	hz	NOUN
eurjchem-1635	179	24	,	,	PUNCT
eurjchem-1635	179	25	ar‐h	ar‐h	NOUN
eurjchem-1635	179	26	)	)	PUNCT
eurjchem-1635	179	27	,	,	PUNCT
eurjchem-1635	179	28	7.62‐7.60	7.62‐7.60	NUM
eurjchem-1635	179	29	(	(	PUNCT
eurjchem-1635	179	30	d	d	NOUN
eurjchem-1635	179	31	,	,	PUNCT
eurjchem-1635	179	32	2h	2h	NUM
eurjchem-1635	179	33	,	,	PUNCT
eurjchem-1635	179	34	j	j	PROPN
eurjchem-1635	179	35	=	=	PROPN
eurjchem-1635	179	36	8.4	8.4	NUM
eurjchem-1635	179	37	hz	hz	NOUN
eurjchem-1635	179	38	,	,	PUNCT
eurjchem-1635	179	39	ar‐h	ar‐h	PROPN
eurjchem-1635	179	40	)	)	PUNCT
eurjchem-1635	179	41	,	,	PUNCT
eurjchem-1635	179	42	7.31‐7.27	7.31‐7.27	NUM
eurjchem-1635	179	43	(	(	PUNCT
eurjchem-1635	179	44	m	m	PROPN
eurjchem-1635	179	45	,	,	PUNCT
eurjchem-1635	179	46	2h	2h	NUM
eurjchem-1635	179	47	,	,	PUNCT
eurjchem-1635	179	48	ar‐h	ar‐h	NOUN
eurjchem-1635	179	49	)	)	PUNCT
eurjchem-1635	179	50	,	,	PUNCT
eurjchem-1635	179	51	7.23‐7.19	7.23‐7.19	NUM
eurjchem-1635	179	52	(	(	PUNCT
eurjchem-1635	179	53	m	m	PROPN
eurjchem-1635	179	54	,	,	PUNCT
eurjchem-1635	179	55	3h	3h	NUM
eurjchem-1635	179	56	,	,	PUNCT
eurjchem-1635	179	57	ar‐h	ar‐h	NOUN
eurjchem-1635	179	58	)	)	PUNCT
eurjchem-1635	179	59	,	,	PUNCT
eurjchem-1635	179	60	6.67‐6.64	6.67‐6.64	NUM
eurjchem-1635	179	61	(	(	PUNCT
eurjchem-1635	179	62	m	m	PROPN
eurjchem-1635	179	63	,	,	PUNCT
eurjchem-1635	179	64	1h	1h	NUM
eurjchem-1635	179	65	,	,	PUNCT
eurjchem-1635	179	66	ar‐h	ar‐h	NOUN
eurjchem-1635	179	67	)	)	PUNCT
eurjchem-1635	179	68	,	,	PUNCT
eurjchem-1635	179	69	6.58	6.58	NUM
eurjchem-1635	179	70	(	(	PUNCT
eurjchem-1635	179	71	d	d	PROPN
eurjchem-1635	179	72	,	,	PUNCT
eurjchem-1635	179	73	2h	2h	NUM
eurjchem-1635	179	74	,	,	PUNCT
eurjchem-1635	179	75	j	j	PROPN
eurjchem-1635	179	76	=	=	SYM
eurjchem-1635	179	77	9.2	9.2	NUM
eurjchem-1635	179	78	hz	hz	NOUN
eurjchem-1635	179	79	,	,	PUNCT
eurjchem-1635	179	80	ar‐h	ar‐h	PROPN
eurjchem-1635	179	81	)	)	PUNCT
eurjchem-1635	179	82	,	,	PUNCT
eurjchem-1635	179	83	6.49	6.49	NUM
eurjchem-1635	179	84	(	(	PUNCT
eurjchem-1635	179	85	t	t	PROPN
eurjchem-1635	179	86	,	,	PUNCT
eurjchem-1635	179	87	1h	1h	NUM
eurjchem-1635	179	88	,	,	PUNCT
eurjchem-1635	179	89	j	j	PROPN
eurjchem-1635	179	90	=	=	SYM
eurjchem-1635	179	91	7.2	7.2	NUM
eurjchem-1635	179	92	hz	hz	NOUN
eurjchem-1635	179	93	,	,	PUNCT
eurjchem-1635	179	94	ar‐h	ar‐h	PROPN
eurjchem-1635	179	95	)	)	PUNCT
eurjchem-1635	179	96	,	,	PUNCT
eurjchem-1635	179	97	4.35	4.35	NUM
eurjchem-1635	179	98	(	(	PUNCT
eurjchem-1635	179	99	m	m	PROPN
eurjchem-1635	179	100	,	,	PUNCT
eurjchem-1635	179	101	2h	2h	NUM
eurjchem-1635	179	102	,	,	PUNCT
eurjchem-1635	179	103	ch2‐ch	ch2‐ch	PRON
eurjchem-1635	179	104	,	,	PUNCT
eurjchem-1635	179	105	s‐ch2	s‐ch2	PROPN
eurjchem-1635	179	106	)	)	PUNCT
eurjchem-1635	179	107	,	,	PUNCT
eurjchem-1635	179	108	4.08	4.08	NUM
eurjchem-1635	179	109	(	(	PUNCT
eurjchem-1635	179	110	q	q	NOUN
eurjchem-1635	179	111	,	,	PUNCT
eurjchem-1635	179	112	1h	1h	NUM
eurjchem-1635	179	113	,	,	PUNCT
eurjchem-1635	179	114	s‐ch2	s‐ch2	PROPN
eurjchem-1635	179	115	)	)	PUNCT
eurjchem-1635	179	116	,	,	PUNCT
eurjchem-1635	179	117	3.30‐	3.30‐	NUM
eurjchem-1635	179	118	3.28	3.28	NUM
eurjchem-1635	179	119	(	(	PUNCT
eurjchem-1635	179	120	dd	dd	PROPN
eurjchem-1635	179	121	,	,	PUNCT
eurjchem-1635	179	122	1h	1h	NUM
eurjchem-1635	179	123	,	,	PUNCT
eurjchem-1635	179	124	n‐ch2	n‐ch2	PROPN
eurjchem-1635	179	125	)	)	PUNCT
eurjchem-1635	179	126	,	,	PUNCT
eurjchem-1635	179	127	3.14‐3.08	3.14‐3.08	NUM
eurjchem-1635	179	128	(	(	PUNCT
eurjchem-1635	179	129	m	m	PROPN
eurjchem-1635	179	130	,	,	PUNCT
eurjchem-1635	179	131	1h	1h	NUM
eurjchem-1635	179	132	,	,	PUNCT
eurjchem-1635	179	133	n‐ch2	n‐ch2	PROPN
eurjchem-1635	179	134	)	)	PUNCT
eurjchem-1635	179	135	,	,	PUNCT
eurjchem-1635	179	136	3.03	3.03	NUM
eurjchem-1635	179	137	(	(	PUNCT
eurjchem-1635	179	138	d	d	PROPN
eurjchem-1635	179	139	,	,	PUNCT
eurjchem-1635	179	140	2h	2h	NUM
eurjchem-1635	179	141	,	,	PUNCT
eurjchem-1635	179	142	j	j	PROPN
eurjchem-1635	179	143	=	=	SYM
eurjchem-1635	179	144	4.4	4.4	NUM
eurjchem-1635	179	145	hz	hz	VERB
eurjchem-1635	179	146	,	,	PUNCT
eurjchem-1635	179	147	ch‐ch2	ch‐ch2	PROPN
eurjchem-1635	179	148	)	)	PUNCT
eurjchem-1635	179	149	.	.	PUNCT
eurjchem-1635	180	1	13c	13c	NOUN
eurjchem-1635	180	2	nmr	nmr	NOUN
eurjchem-1635	180	3	(	(	PUNCT
eurjchem-1635	180	4	100	100	NUM
eurjchem-1635	180	5	mhz	mhz	NOUN
eurjchem-1635	180	6	,	,	PUNCT
eurjchem-1635	180	7	cdcl3	cdcl3	PROPN
eurjchem-1635	180	8	,	,	PUNCT
eurjchem-1635	180	9	δ	δ	PROPN
eurjchem-1635	180	10	,	,	PUNCT
eurjchem-1635	180	11	ppm	ppm	NOUN
eurjchem-1635	180	12	):	):	PUNCT
eurjchem-1635	180	13	141.12	141.12	NUM
eurjchem-1635	180	14	,	,	PUNCT
eurjchem-1635	180	15	140.21	140.21	NUM
eurjchem-1635	180	16	,	,	PUNCT
eurjchem-1635	180	17	139.38	139.38	NUM
eurjchem-1635	180	18	,	,	PUNCT
eurjchem-1635	180	19	135.36	135.36	NUM
eurjchem-1635	180	20	,	,	PUNCT
eurjchem-1635	180	21	129.26	129.26	NUM
eurjchem-1635	180	22	,	,	PUNCT
eurjchem-1635	180	23	128.78	128.78	NUM
eurjchem-1635	180	24	,	,	PUNCT
eurjchem-1635	180	25	128.72	128.72	NUM
eurjchem-1635	180	26	,	,	PUNCT
eurjchem-1635	180	27	127.66	127.66	NUM
eurjchem-1635	180	28	,	,	PUNCT
eurjchem-1635	180	29	127.11	127.11	NUM
eurjchem-1635	180	30	,	,	PUNCT
eurjchem-1635	180	31	127.10	127.10	NUM
eurjchem-1635	180	32	,	,	PUNCT
eurjchem-1635	180	33	127.01	127.01	NUM
eurjchem-1635	180	34	,	,	PUNCT
eurjchem-1635	180	35	126.12	126.12	NUM
eurjchem-1635	180	36	,	,	PUNCT
eurjchem-1635	180	37	125.11	125.11	NUM
eurjchem-1635	180	38	,	,	PUNCT
eurjchem-1635	180	39	125.10	125.10	NUM
eurjchem-1635	180	40	,	,	PUNCT
eurjchem-1635	180	41	115.12	115.12	NUM
eurjchem-1635	180	42	,	,	PUNCT
eurjchem-1635	180	43	115.10	115.10	NUM
eurjchem-1635	180	44	,	,	PUNCT
eurjchem-1635	180	45	110.22	110.22	NUM
eurjchem-1635	180	46	,	,	PUNCT
eurjchem-1635	180	47	110.14	110.14	NUM
eurjchem-1635	180	48	,	,	PUNCT
eurjchem-1635	180	49	78.31	78.31	NUM
eurjchem-1635	180	50	,	,	PUNCT
eurjchem-1635	180	51	54.12	54.12	NUM
eurjchem-1635	180	52	,	,	PUNCT
eurjchem-1635	180	53	38.25	38.25	NUM
eurjchem-1635	180	54	,	,	PUNCT
eurjchem-1635	180	55	38.11	38.11	NUM
eurjchem-1635	180	56	.	.	PUNCT
eurjchem-1635	181	1	ms	ms	NOUN
eurjchem-1635	181	2	(	(	PUNCT
eurjchem-1635	181	3	ei	ei	PROPN
eurjchem-1635	181	4	,	,	PUNCT
eurjchem-1635	181	5	m	m	PROPN
eurjchem-1635	181	6	/	/	SYM
eurjchem-1635	181	7	z	z	PROPN
eurjchem-1635	181	8	(	(	PUNCT
eurjchem-1635	181	9	%	%	NOUN
eurjchem-1635	181	10	)	)	PUNCT
eurjchem-1635	181	11	):	):	PUNCT
eurjchem-1635	181	12	447	447	NUM
eurjchem-1635	182	1	[	[	X
eurjchem-1635	182	2	m+h	m+h	NOUN
eurjchem-1635	182	3	]	]	PUNCT
eurjchem-1635	182	4	.	.	PUNCT
eurjchem-1635	183	1	hplc	hplc	NOUN
eurjchem-1635	183	2	:	:	PUNCT
eurjchem-1635	183	3	purity	purity	NOUN
eurjchem-1635	183	4	=	=	SYM
eurjchem-1635	183	5	97.4	97.4	NUM
eurjchem-1635	183	6	%	%	NOUN
eurjchem-1635	183	7	,	,	PUNCT
eurjchem-1635	183	8	r.t	r.t	PROPN
eurjchem-1635	183	9	.	.	PUNCT
eurjchem-1635	184	1	=	=	PROPN
eurjchem-1635	184	2	8.12	8.12	NUM
eurjchem-1635	184	3	min	min	NOUN
eurjchem-1635	184	4	.	.	PROPN
eurjchem-1635	184	5	2‐((benzylthio)methyl)‐4‐((4‐(trifluoromethyl)phenyl	2‐((benzylthio)methyl)‐4‐((4‐(trifluoromethyl)phenyl	NUM
eurjchem-1635	184	6	)	)	PUNCT
eurjchem-1635	184	7	sul‐	sul‐	X
eurjchem-1635	184	8	fonyl)‐3,4‐dihydro‐2h‐benzo[b][1,4]oxazine	fonyl)‐3,4‐dihydro‐2h‐benzo[b][1,4]oxazine	X
eurjchem-1635	184	9	(	(	PUNCT
eurjchem-1635	184	10	7d	7d	NUM
eurjchem-1635	184	11	):	):	PUNCT
eurjchem-1635	184	12	color	color	NOUN
eurjchem-1635	184	13	:	:	PUNCT
eurjchem-1635	184	14	white	white	ADJ
eurjchem-1635	184	15	.	.	PUNCT
eurjchem-1635	184	16	yield	yield	NOUN
eurjchem-1635	184	17	:	:	PUNCT
eurjchem-1635	184	18	86	86	NUM
eurjchem-1635	184	19	%	%	NOUN
eurjchem-1635	184	20	.	.	PUNCT
eurjchem-1635	185	1	m.p	m.p	PROPN
eurjchem-1635	185	2	.	.	PROPN
eurjchem-1635	185	3	:	:	PUNCT
eurjchem-1635	186	1	191‐192	191‐192	NUM
eurjchem-1635	186	2	°	°	ADP
eurjchem-1635	186	3	c	c	NOUN
eurjchem-1635	186	4	.	.	PUNCT
eurjchem-1635	187	1	1h	1h	NUM
eurjchem-1635	187	2	nmr	nmr	NOUN
eurjchem-1635	187	3	(	(	PUNCT
eurjchem-1635	187	4	400	400	NUM
eurjchem-1635	187	5	mhz	mhz	NOUN
eurjchem-1635	187	6	,	,	PUNCT
eurjchem-1635	187	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	187	8	,	,	PUNCT
eurjchem-1635	187	9	δ	δ	PROPN
eurjchem-1635	187	10	,	,	PUNCT
eurjchem-1635	187	11	ppm	ppm	NUM
eurjchem-1635	187	12	):	):	PUNCT
eurjchem-1635	187	13	7.80‐7.71	7.80‐7.71	NUM
eurjchem-1635	187	14	(	(	PUNCT
eurjchem-1635	187	15	d	d	NOUN
eurjchem-1635	187	16	,	,	PUNCT
eurjchem-1635	187	17	2h	2h	NUM
eurjchem-1635	187	18	,	,	PUNCT
eurjchem-1635	187	19	j	j	PROPN
eurjchem-1635	187	20	=	=	PROPN
eurjchem-1635	187	21	8.4	8.4	NUM
eurjchem-1635	187	22	hz	hz	NOUN
eurjchem-1635	187	23	,	,	PUNCT
eurjchem-1635	187	24	ar‐h	ar‐h	PROPN
eurjchem-1635	187	25	)	)	PUNCT
eurjchem-1635	187	26	,	,	PUNCT
eurjchem-1635	187	27	7.66‐7.44	7.66‐7.44	NUM
eurjchem-1635	187	28	(	(	PUNCT
eurjchem-1635	187	29	d	d	PROPN
eurjchem-1635	187	30	,	,	PUNCT
eurjchem-1635	187	31	2h	2h	NUM
eurjchem-1635	187	32	,	,	PUNCT
eurjchem-1635	187	33	j	j	PROPN
eurjchem-1635	187	34	=	=	PROPN
eurjchem-1635	187	35	8.4	8.4	NUM
eurjchem-1635	187	36	hz	hz	NOUN
eurjchem-1635	187	37	,	,	PUNCT
eurjchem-1635	187	38	ar‐h	ar‐h	NOUN
eurjchem-1635	187	39	)	)	PUNCT
eurjchem-1635	187	40	,	,	PUNCT
eurjchem-1635	187	41	7.41‐7.37	7.41‐7.37	NUM
eurjchem-1635	187	42	(	(	PUNCT
eurjchem-1635	187	43	m	m	PROPN
eurjchem-1635	187	44	,	,	PUNCT
eurjchem-1635	187	45	2h	2h	NUM
eurjchem-1635	187	46	,	,	PUNCT
eurjchem-1635	187	47	ar‐h	ar‐h	NOUN
eurjchem-1635	187	48	)	)	PUNCT
eurjchem-1635	187	49	,	,	PUNCT
eurjchem-1635	187	50	7.21‐7.18	7.21‐7.18	NUM
eurjchem-1635	187	51	(	(	PUNCT
eurjchem-1635	187	52	m	m	PROPN
eurjchem-1635	187	53	,	,	PUNCT
eurjchem-1635	187	54	3h	3h	NUM
eurjchem-1635	187	55	,	,	PUNCT
eurjchem-1635	187	56	ar‐h	ar‐h	NOUN
eurjchem-1635	187	57	)	)	PUNCT
eurjchem-1635	187	58	,	,	PUNCT
eurjchem-1635	187	59	6.67‐6.64	6.67‐6.64	NUM
eurjchem-1635	187	60	(	(	PUNCT
eurjchem-1635	187	61	m	m	PROPN
eurjchem-1635	187	62	,	,	PUNCT
eurjchem-1635	187	63	2h	2h	NUM
eurjchem-1635	187	64	,	,	PUNCT
eurjchem-1635	187	65	ar‐h	ar‐h	NOUN
eurjchem-1635	187	66	)	)	PUNCT
eurjchem-1635	187	67	,	,	PUNCT
eurjchem-1635	187	68	6.58	6.58	NUM
eurjchem-1635	187	69	(	(	PUNCT
eurjchem-1635	187	70	d	d	PROPN
eurjchem-1635	187	71	,	,	PUNCT
eurjchem-1635	187	72	1h	1h	NUM
eurjchem-1635	187	73	,	,	PUNCT
eurjchem-1635	187	74	j	j	PROPN
eurjchem-1635	187	75	=	=	SYM
eurjchem-1635	187	76	9.2	9.2	NUM
eurjchem-1635	187	77	hz	hz	NOUN
eurjchem-1635	187	78	,	,	PUNCT
eurjchem-1635	187	79	ar‐h	ar‐h	PROPN
eurjchem-1635	187	80	)	)	PUNCT
eurjchem-1635	187	81	,	,	PUNCT
eurjchem-1635	187	82	6.49	6.49	NUM
eurjchem-1635	187	83	(	(	PUNCT
eurjchem-1635	187	84	t	t	PROPN
eurjchem-1635	187	85	,	,	PUNCT
eurjchem-1635	187	86	1h	1h	NUM
eurjchem-1635	187	87	,	,	PUNCT
eurjchem-1635	187	88	j	j	PROPN
eurjchem-1635	187	89	=	=	SYM
eurjchem-1635	187	90	7.2	7.2	NUM
eurjchem-1635	187	91	hz	hz	NOUN
eurjchem-1635	187	92	,	,	PUNCT
eurjchem-1635	187	93	ar‐h	ar‐h	PROPN
eurjchem-1635	187	94	)	)	PUNCT
eurjchem-1635	187	95	,	,	PUNCT
eurjchem-1635	187	96	4.33	4.33	NUM
eurjchem-1635	187	97	(	(	PUNCT
eurjchem-1635	187	98	m	m	PROPN
eurjchem-1635	187	99	,	,	PUNCT
eurjchem-1635	187	100	2h	2h	NUM
eurjchem-1635	187	101	,	,	PUNCT
eurjchem-1635	187	102	ch2‐ch	ch2‐ch	PRON
eurjchem-1635	187	103	,	,	PUNCT
eurjchem-1635	187	104	s‐ch2	s‐ch2	PROPN
eurjchem-1635	187	105	)	)	PUNCT
eurjchem-1635	187	106	,	,	PUNCT
eurjchem-1635	187	107	4.06	4.06	NUM
eurjchem-1635	187	108	(	(	PUNCT
eurjchem-1635	187	109	q	q	NOUN
eurjchem-1635	187	110	,	,	PUNCT
eurjchem-1635	187	111	1h	1h	NUM
eurjchem-1635	187	112	,	,	PUNCT
eurjchem-1635	187	113	s‐ch2	s‐ch2	PROPN
eurjchem-1635	187	114	)	)	PUNCT
eurjchem-1635	187	115	,	,	PUNCT
eurjchem-1635	187	116	3.32‐3.28	3.32‐3.28	NUM
eurjchem-1635	187	117	(	(	PUNCT
eurjchem-1635	187	118	dd	dd	PROPN
eurjchem-1635	187	119	,	,	PUNCT
eurjchem-1635	187	120	1h	1h	NUM
eurjchem-1635	187	121	,	,	PUNCT
eurjchem-1635	187	122	n‐ch2	n‐ch2	PROPN
eurjchem-1635	187	123	)	)	PUNCT
eurjchem-1635	187	124	,	,	PUNCT
eurjchem-1635	187	125	3.16‐3.07	3.16‐3.07	NUM
eurjchem-1635	187	126	(	(	PUNCT
eurjchem-1635	187	127	m	m	PROPN
eurjchem-1635	187	128	,	,	PUNCT
eurjchem-1635	187	129	1h	1h	NUM
eurjchem-1635	187	130	,	,	PUNCT
eurjchem-1635	187	131	n‐ch2	n‐ch2	PROPN
eurjchem-1635	187	132	)	)	PUNCT
eurjchem-1635	187	133	,	,	PUNCT
eurjchem-1635	187	134	3.02	3.02	NUM
eurjchem-1635	187	135	(	(	PUNCT
eurjchem-1635	187	136	d	d	NOUN
eurjchem-1635	187	137	,	,	PUNCT
eurjchem-1635	187	138	2h	2h	NUM
eurjchem-1635	187	139	,	,	PUNCT
eurjchem-1635	187	140	j	j	PROPN
eurjchem-1635	187	141	=	=	SYM
eurjchem-1635	187	142	4.4	4.4	NUM
eurjchem-1635	187	143	hz	hz	VERB
eurjchem-1635	187	144	,	,	PUNCT
eurjchem-1635	187	145	ch‐ch2	ch‐ch2	PROPN
eurjchem-1635	187	146	)	)	PUNCT
eurjchem-1635	187	147	.	.	PUNCT
eurjchem-1635	188	1	13c	13c	NOUN
eurjchem-1635	188	2	nmr	nmr	NOUN
eurjchem-1635	188	3	(	(	PUNCT
eurjchem-1635	188	4	100	100	NUM
eurjchem-1635	188	5	mhz	mhz	NOUN
eurjchem-1635	188	6	,	,	PUNCT
eurjchem-1635	188	7	cdcl3	cdcl3	PROPN
eurjchem-1635	188	8	,	,	PUNCT
eurjchem-1635	188	9	δ	δ	PROPN
eurjchem-1635	188	10	,	,	PUNCT
eurjchem-1635	188	11	ppm	ppm	NOUN
eurjchem-1635	188	12	):	):	PUNCT
eurjchem-1635	188	13	141.12	141.12	NUM
eurjchem-1635	188	14	,	,	PUNCT
eurjchem-1635	188	15	140.10	140.10	NUM
eurjchem-1635	188	16	,	,	PUNCT
eurjchem-1635	188	17	139.48	139.48	NUM
eurjchem-1635	188	18	,	,	PUNCT
eurjchem-1635	188	19	135.26	135.26	NUM
eurjchem-1635	188	20	,	,	PUNCT
eurjchem-1635	188	21	129.26	129.26	NUM
eurjchem-1635	188	22	,	,	PUNCT
eurjchem-1635	188	23	128.78	128.78	NUM
eurjchem-1635	188	24	,	,	PUNCT
eurjchem-1635	188	25	128.22	128.22	NUM
eurjchem-1635	188	26	,	,	PUNCT
eurjchem-1635	188	27	127.66	127.66	NUM
eurjchem-1635	188	28	,	,	PUNCT
eurjchem-1635	188	29	127.11	127.11	NUM
eurjchem-1635	188	30	,	,	PUNCT
eurjchem-1635	188	31	127.10	127.10	NUM
eurjchem-1635	188	32	,	,	PUNCT
eurjchem-1635	188	33	127.01	127.01	NUM
eurjchem-1635	188	34	,	,	PUNCT
eurjchem-1635	188	35	126.12	126.12	NUM
eurjchem-1635	188	36	,	,	PUNCT
eurjchem-1635	188	37	125.26	125.26	NUM
eurjchem-1635	188	38	,	,	PUNCT
eurjchem-1635	188	39	125.11	125.11	NUM
eurjchem-1635	188	40	,	,	PUNCT
eurjchem-1635	188	41	125.10	125.10	NUM
eurjchem-1635	188	42	,	,	PUNCT
eurjchem-1635	188	43	115.12	115.12	NUM
eurjchem-1635	188	44	,	,	PUNCT
eurjchem-1635	188	45	115.10	115.10	NUM
eurjchem-1635	188	46	,	,	PUNCT
eurjchem-1635	188	47	110.22	110.22	NUM
eurjchem-1635	188	48	,	,	PUNCT
eurjchem-1635	188	49	110.14	110.14	NUM
eurjchem-1635	188	50	,	,	PUNCT
eurjchem-1635	188	51	78.31	78.31	NUM
eurjchem-1635	188	52	,	,	PUNCT
eurjchem-1635	188	53	54.12	54.12	NUM
eurjchem-1635	188	54	,	,	PUNCT
eurjchem-1635	188	55	38.15	38.15	NUM
eurjchem-1635	188	56	,	,	PUNCT
eurjchem-1635	188	57	38.11	38.11	NUM
eurjchem-1635	188	58	.	.	PUNCT
eurjchem-1635	189	1	ms	ms	NOUN
eurjchem-1635	189	2	(	(	PUNCT
eurjchem-1635	189	3	ei	ei	PROPN
eurjchem-1635	189	4	,	,	PUNCT
eurjchem-1635	189	5	m	m	PROPN
eurjchem-1635	189	6	/	/	SYM
eurjchem-1635	189	7	z	z	PROPN
eurjchem-1635	189	8	(	(	PUNCT
eurjchem-1635	189	9	%	%	NOUN
eurjchem-1635	189	10	)	)	PUNCT
eurjchem-1635	189	11	):	):	PUNCT
eurjchem-1635	189	12	480	480	NUM
eurjchem-1635	190	1	[	[	X
eurjchem-1635	190	2	m+h	m+h	NOUN
eurjchem-1635	190	3	]	]	X
eurjchem-1635	190	4	.	.	PUNCT
eurjchem-1635	191	1	hplc	hplc	NOUN
eurjchem-1635	191	2	:	:	PUNCT
eurjchem-1635	191	3	purity	purity	NOUN
eurjchem-1635	191	4	=	=	NOUN
eurjchem-1635	191	5	98.4	98.4	NUM
eurjchem-1635	191	6	%	%	NOUN
eurjchem-1635	191	7	,	,	PUNCT
eurjchem-1635	191	8	r.t	r.t	PROPN
eurjchem-1635	191	9	.	.	PUNCT
eurjchem-1635	191	10	=	=	NOUN
eurjchem-1635	191	11	8.38	8.38	NUM
eurjchem-1635	191	12	min	min	NOUN
eurjchem-1635	191	13	.	.	PROPN
eurjchem-1635	191	14	2‐((benzylthio)methyl)‐4‐(methylsulfonyl)‐3	2‐((benzylthio)methyl)‐4‐(methylsulfonyl)‐3	NUM
eurjchem-1635	191	15	,	,	PUNCT
eurjchem-1635	191	16	4‐dihydro‐2h‐	4‐dihydro‐2h‐	PROPN
eurjchem-1635	191	17	benzo[b][1,4]oxazine	benzo[b][1,4]oxazine	NOUN
eurjchem-1635	191	18	(	(	PUNCT
eurjchem-1635	191	19	7e	7e	NUM
eurjchem-1635	191	20	):	):	PUNCT
eurjchem-1635	191	21	color	color	NOUN
eurjchem-1635	191	22	:	:	PUNCT
eurjchem-1635	191	23	yellow	yellow	ADJ
eurjchem-1635	191	24	.	.	PUNCT
eurjchem-1635	192	1	yield	yield	NOUN
eurjchem-1635	192	2	:	:	PUNCT
eurjchem-1635	192	3	81	81	NUM
eurjchem-1635	192	4	%	%	NOUN
eurjchem-1635	192	5	.	.	PUNCT
eurjchem-1635	193	1	m.p	m.p	PROPN
eurjchem-1635	193	2	.	.	PROPN
eurjchem-1635	193	3	:	:	PUNCT
eurjchem-1635	194	1	127‐	127‐	NUM
eurjchem-1635	194	2	128	128	NUM
eurjchem-1635	194	3	°	°	NOUN
eurjchem-1635	194	4	c	c	NOUN
eurjchem-1635	194	5	.	.	PUNCT
eurjchem-1635	195	1	1h	1h	NUM
eurjchem-1635	195	2	nmr	nmr	NOUN
eurjchem-1635	195	3	(	(	PUNCT
eurjchem-1635	195	4	400	400	NUM
eurjchem-1635	195	5	mhz	mhz	NOUN
eurjchem-1635	195	6	,	,	PUNCT
eurjchem-1635	195	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-1635	195	8	,	,	PUNCT
eurjchem-1635	195	9	δ	δ	PROPN
eurjchem-1635	195	10	,	,	PUNCT
eurjchem-1635	195	11	ppm	ppm	NUM
eurjchem-1635	195	12	):	):	PUNCT
eurjchem-1635	195	13	7.30‐7.18	7.30‐7.18	NOUN
eurjchem-1635	195	14	(	(	PUNCT
eurjchem-1635	195	15	br	br	PROPN
eurjchem-1635	195	16	m	m	PROPN
eurjchem-1635	195	17	,	,	PUNCT
eurjchem-1635	195	18	5h	5h	NUM
eurjchem-1635	195	19	,	,	PUNCT
eurjchem-1635	195	20	ar‐h	ar‐h	NOUN
eurjchem-1635	195	21	)	)	PUNCT
eurjchem-1635	195	22	,	,	PUNCT
eurjchem-1635	195	23	6.74‐6.67	6.74‐6.67	NUM
eurjchem-1635	195	24	(	(	PUNCT
eurjchem-1635	195	25	m	m	PROPN
eurjchem-1635	195	26	,	,	PUNCT
eurjchem-1635	195	27	3h	3h	NUM
eurjchem-1635	195	28	,	,	PUNCT
eurjchem-1635	195	29	ar‐h	ar‐h	NOUN
eurjchem-1635	195	30	)	)	PUNCT
eurjchem-1635	195	31	,	,	PUNCT
eurjchem-1635	195	32	6.54	6.54	NUM
eurjchem-1635	195	33	(	(	PUNCT
eurjchem-1635	195	34	t	t	PROPN
eurjchem-1635	195	35	,	,	PUNCT
eurjchem-1635	195	36	1h	1h	NUM
eurjchem-1635	195	37	,	,	PUNCT
eurjchem-1635	195	38	ar‐h	ar‐h	NOUN
eurjchem-1635	195	39	)	)	PUNCT
eurjchem-1635	195	40	,	,	PUNCT
eurjchem-1635	195	41	4.46‐4,32	4.46‐4,32	NUM
eurjchem-1635	195	42	(	(	PUNCT
eurjchem-1635	195	43	m	m	PROPN
eurjchem-1635	195	44	,	,	PUNCT
eurjchem-1635	195	45	2h	2h	NUM
eurjchem-1635	195	46	,	,	PUNCT
eurjchem-1635	195	47	ch2‐ch	ch2‐ch	PRON
eurjchem-1635	195	48	,	,	PUNCT
eurjchem-1635	195	49	s‐ch2	s‐ch2	PROPN
eurjchem-1635	195	50	)	)	PUNCT
eurjchem-1635	195	51	,	,	PUNCT
eurjchem-1635	195	52	4.16	4.16	NUM
eurjchem-1635	195	53	(	(	PUNCT
eurjchem-1635	195	54	q	q	NOUN
eurjchem-1635	195	55	,	,	PUNCT
eurjchem-1635	195	56	1h	1h	NUM
eurjchem-1635	195	57	,	,	PUNCT
eurjchem-1635	195	58	s‐ch2	s‐ch2	PROPN
eurjchem-1635	195	59	)	)	PUNCT
eurjchem-1635	195	60	,	,	PUNCT
eurjchem-1635	195	61	3.36‐3.33	3.36‐3.33	NUM
eurjchem-1635	195	62	(	(	PUNCT
eurjchem-1635	195	63	dd	dd	PROPN
eurjchem-1635	195	64	,	,	PUNCT
eurjchem-1635	195	65	1h	1h	NUM
eurjchem-1635	195	66	,	,	PUNCT
eurjchem-1635	195	67	n‐ch2	n‐ch2	PROPN
eurjchem-1635	195	68	)	)	PUNCT
eurjchem-1635	195	69	,	,	PUNCT
eurjchem-1635	195	70	3.19‐3.13	3.19‐3.13	NUM
eurjchem-1635	195	71	(	(	PUNCT
eurjchem-1635	195	72	m	m	PROPN
eurjchem-1635	195	73	,	,	PUNCT
eurjchem-1635	195	74	3h	3h	NUM
eurjchem-1635	195	75	,	,	PUNCT
eurjchem-1635	195	76	n‐ch2	n‐ch2	NOUN
eurjchem-1635	195	77	,	,	PUNCT
eurjchem-1635	195	78	ch‐ch2	ch‐ch2	PROPN
eurjchem-1635	195	79	)	)	PUNCT
eurjchem-1635	195	80	,	,	PUNCT
eurjchem-1635	195	81	2.89	2.89	NUM
eurjchem-1635	195	82	(	(	PUNCT
eurjchem-1635	195	83	s	s	PROPN
eurjchem-1635	195	84	,	,	PUNCT
eurjchem-1635	195	85	3h	3h	NUM
eurjchem-1635	195	86	,	,	PUNCT
eurjchem-1635	195	87	s‐ch3	s‐ch3	PROPN
eurjchem-1635	195	88	)	)	PUNCT
eurjchem-1635	195	89	.	.	PUNCT
eurjchem-1635	196	1	13c	13c	NOUN
eurjchem-1635	196	2	nmr	nmr	NOUN
eurjchem-1635	196	3	(	(	PUNCT
eurjchem-1635	196	4	100	100	NUM
eurjchem-1635	196	5	mhz	mhz	NOUN
eurjchem-1635	196	6	,	,	PUNCT
eurjchem-1635	196	7	cdcl3	cdcl3	PROPN
eurjchem-1635	196	8	,	,	PUNCT
eurjchem-1635	196	9	δ	δ	PROPN
eurjchem-1635	196	10	,	,	PUNCT
eurjchem-1635	196	11	ppm	ppm	NOUN
eurjchem-1635	196	12	):	):	PUNCT
eurjchem-1635	196	13	141.12	141.12	NUM
eurjchem-1635	196	14	,	,	PUNCT
eurjchem-1635	196	15	140.11	140.11	NUM
eurjchem-1635	196	16	,	,	PUNCT
eurjchem-1635	196	17	139.38	139.38	NUM
eurjchem-1635	196	18	,	,	PUNCT
eurjchem-1635	196	19	135.36	135.36	NUM
eurjchem-1635	196	20	,	,	PUNCT
eurjchem-1635	196	21	129.20	129.20	NUM
eurjchem-1635	196	22	,	,	PUNCT
eurjchem-1635	196	23	128.78	128.78	NUM
eurjchem-1635	196	24	,	,	PUNCT
eurjchem-1635	196	25	128.12	128.12	NUM
eurjchem-1635	196	26	,	,	PUNCT
eurjchem-1635	196	27	127.10	127.10	NUM
eurjchem-1635	196	28	,	,	PUNCT
eurjchem-1635	196	29	127.01	127.01	NUM
eurjchem-1635	196	30	,	,	PUNCT
eurjchem-1635	196	31	125.10	125.10	NUM
eurjchem-1635	196	32	,	,	PUNCT
eurjchem-1635	196	33	115.12	115.12	NUM
eurjchem-1635	196	34	,	,	PUNCT
eurjchem-1635	196	35	115.10	115.10	NUM
eurjchem-1635	196	36	,	,	PUNCT
eurjchem-1635	196	37	110.22	110.22	NUM
eurjchem-1635	196	38	,	,	PUNCT
eurjchem-1635	196	39	110.14	110.14	NUM
eurjchem-1635	196	40	,	,	PUNCT
eurjchem-1635	196	41	78.3	78.3	NUM
eurjchem-1635	196	42	,	,	PUNCT
eurjchem-1635	196	43	54.12	54.12	NUM
eurjchem-1635	196	44	,	,	PUNCT
eurjchem-1635	196	45	38.15	38.15	NUM
eurjchem-1635	196	46	,	,	PUNCT
eurjchem-1635	196	47	38.10	38.10	NUM
eurjchem-1635	196	48	,	,	PUNCT
eurjchem-1635	196	49	37.28	37.28	NUM
eurjchem-1635	196	50	.	.	PUNCT
eurjchem-1635	197	1	ms	ms	NOUN
eurjchem-1635	197	2	(	(	PUNCT
eurjchem-1635	197	3	ei	ei	PROPN
eurjchem-1635	197	4	,	,	PUNCT
eurjchem-1635	197	5	m	m	PROPN
eurjchem-1635	197	6	/	/	SYM
eurjchem-1635	197	7	z	z	PROPN
eurjchem-1635	197	8	(	(	PUNCT
eurjchem-1635	197	9	%	%	NOUN
eurjchem-1635	197	10	)	)	PUNCT
eurjchem-1635	197	11	):	):	PUNCT
eurjchem-1635	197	12	350	350	NUM
eurjchem-1635	197	13	[	[	X
eurjchem-1635	197	14	m+h	m+h	NOUN
eurjchem-1635	197	15	]	]	PUNCT
eurjchem-1635	197	16	.	.	PUNCT
eurjchem-1635	198	1	hplc	hplc	NOUN
eurjchem-1635	198	2	:	:	PUNCT
eurjchem-1635	198	3	purity	purity	NOUN
eurjchem-1635	198	4	=	=	NOUN
eurjchem-1635	198	5	98.4	98.4	NUM
eurjchem-1635	198	6	%	%	NOUN
eurjchem-1635	198	7	,	,	PUNCT
eurjchem-1635	198	8	r.t	r.t	PROPN
eurjchem-1635	198	9	.	.	PUNCT
eurjchem-1635	198	10	=	=	NOUN
eurjchem-1635	198	11	7.64	7.64	NUM
eurjchem-1635	198	12	min	min	NOUN
eurjchem-1635	198	13	.	.	PROPN
eurjchem-1635	198	14	2.3	2.3	NUM
eurjchem-1635	198	15	.	.	PUNCT
eurjchem-1635	199	1	anticancer	anticancer	NOUN
eurjchem-1635	199	2	activity	activity	NOUN
eurjchem-1635	199	3	all	all	DET
eurjchem-1635	199	4	the	the	DET
eurjchem-1635	199	5	synthesized	synthesize	VERB
eurjchem-1635	199	6	compounds	compound	NOUN
eurjchem-1635	199	7	were	be	AUX
eurjchem-1635	199	8	tested	test	VERB
eurjchem-1635	199	9	for	for	ADP
eurjchem-1635	199	10	their	their	PRON
eurjchem-1635	199	11	in	in	ADP
eurjchem-1635	199	12	vitro	vitro	X
eurjchem-1635	199	13	anticancer	anticancer	NOUN
eurjchem-1635	199	14	activity	activity	NOUN
eurjchem-1635	199	15	against	against	ADP
eurjchem-1635	199	16	a‐549‐human	a‐549‐human	PROPN
eurjchem-1635	199	17	lung	lung	NOUN
eurjchem-1635	199	18	cancer	cancer	NOUN
eurjchem-1635	199	19	cell	cell	NOUN
eurjchem-1635	199	20	line	line	NOUN
eurjchem-1635	199	21	,	,	PUNCT
eurjchem-1635	199	22	hela‐human	hela‐human	NOUN
eurjchem-1635	199	23	cervical	cervical	ADJ
eurjchem-1635	199	24	cancer	cancer	NOUN
eurjchem-1635	199	25	cell	cell	NOUN
eurjchem-1635	199	26	line	line	NOUN
eurjchem-1635	199	27	,	,	PUNCT
eurjchem-1635	199	28	mcf‐7‐human	mcf‐7‐human	PROPN
eurjchem-1635	199	29	breast	breast	NOUN
eurjchem-1635	199	30	cancer	cancer	NOUN
eurjchem-1635	199	31	cell	cell	NOUN
eurjchem-1635	199	32	line	line	NOUN
eurjchem-1635	199	33	,	,	PUNCT
eurjchem-1635	199	34	du‐145‐human	du‐145‐human	NOUN
eurjchem-1635	199	35	prostate	prostate	NOUN
eurjchem-1635	199	36	cancer	cancer	NOUN
eurjchem-1635	199	37	cell	cell	NOUN
eurjchem-1635	199	38	line	line	NOUN
eurjchem-1635	199	39	and	and	CCONJ
eurjchem-1635	199	40	huvec‐human	huvec‐human	ADJ
eurjchem-1635	199	41	umbilical	umbilical	ADJ
eurjchem-1635	199	42	vein	vein	ADJ
eurjchem-1635	199	43	endothelial	endothelial	ADJ
eurjchem-1635	199	44	cell	cell	NOUN
eurjchem-1635	199	45	line	line	NOUN
eurjchem-1635	199	46	.	.	PUNCT
eurjchem-1635	200	1	the	the	DET
eurjchem-1635	200	2	anticancer	anticancer	NOUN
eurjchem-1635	200	3	activity	activity	NOUN
eurjchem-1635	200	4	test	test	NOUN
eurjchem-1635	200	5	is	be	AUX
eurjchem-1635	200	6	performed	perform	VERB
eurjchem-1635	200	7	according	accord	VERB
eurjchem-1635	200	8	to	to	ADP
eurjchem-1635	200	9	the	the	DET
eurjchem-1635	200	10	procedure	procedure	NOUN
eurjchem-1635	200	11	developed	develop	VERB
eurjchem-1635	200	12	by	by	ADP
eurjchem-1635	200	13	the	the	DET
eurjchem-1635	200	14	national	national	PROPN
eurjchem-1635	200	15	cancer	cancer	PROPN
eurjchem-1635	200	16	institute	institute	PROPN
eurjchem-1635	200	17	(	(	PUNCT
eurjchem-1635	200	18	nci	nci	PROPN
eurjchem-1635	200	19	,	,	PUNCT
eurjchem-1635	200	20	usa	usa	PROPN
eurjchem-1635	200	21	)	)	PUNCT
eurjchem-1635	200	22	in	in	ADP
eurjchem-1635	200	23	the	the	DET
eurjchem-1635	200	24	‘	'	PUNCT
eurjchem-1635	200	25	in	in	X
eurjchem-1635	200	26	vitro	vitro	X
eurjchem-1635	200	27	anticancer	anticancer	NOUN
eurjchem-1635	200	28	drug	drug	NOUN
eurjchem-1635	200	29	discovery	discovery	PROPN
eurjchem-1635	200	30	screen	screen	NOUN
eurjchem-1635	200	31	’	'	PUNCT
eurjchem-1635	200	32	that	that	PRON
eurjchem-1635	200	33	uses	use	VERB
eurjchem-1635	200	34	the	the	DET
eurjchem-1635	200	35	protein‐binding	protein‐binde	VERB
eurjchem-1635	200	36	dye	dye	NOUN
eurjchem-1635	200	37	sulforhodamine	sulforhodamine	NOUN
eurjchem-1635	200	38	b	b	PROPN
eurjchem-1635	200	39	(	(	PUNCT
eurjchem-1635	200	40	srb	srb	PROPN
eurjchem-1635	200	41	)	)	PUNCT
eurjchem-1635	200	42	to	to	PART
eurjchem-1635	200	43	assess	assess	VERB
eurjchem-1635	200	44	cell	cell	NOUN
eurjchem-1635	200	45	growth	growth	NOUN
eurjchem-1635	200	46	[	[	X
eurjchem-1635	200	47	23,24	23,24	NOUN
eurjchem-1635	200	48	]	]	PUNCT
eurjchem-1635	200	49	.	.	PUNCT
eurjchem-1635	201	1	briefly	briefly	NOUN
eurjchem-1635	201	2	,	,	PUNCT
eurjchem-1635	201	3	cells	cell	NOUN
eurjchem-1635	201	4	are	be	AUX
eurjchem-1635	201	5	grown	grow	VERB
eurjchem-1635	201	6	in	in	ADP
eurjchem-1635	201	7	96‐well	96‐well	NUM
eurjchem-1635	201	8	plates	plate	NOUN
eurjchem-1635	201	9	in	in	ADP
eurjchem-1635	201	10	suspension	suspension	NOUN
eurjchem-1635	201	11	and	and	CCONJ
eurjchem-1635	201	12	then	then	ADV
eurjchem-1635	201	13	were	be	AUX
eurjchem-1635	201	14	exposed	expose	VERB
eurjchem-1635	201	15	for	for	ADP
eurjchem-1635	201	16	48	48	NUM
eurjchem-1635	201	17	hours	hour	NOUN
eurjchem-1635	201	18	to	to	ADP
eurjchem-1635	201	19	four	four	NUM
eurjchem-1635	201	20	serial	serial	ADJ
eurjchem-1635	201	21	concentrations	concentration	NOUN
eurjchem-1635	201	22	of	of	ADP
eurjchem-1635	201	23	1×10‐7	1×10‐7	NUM
eurjchem-1635	201	24	,	,	PUNCT
eurjchem-1635	201	25	1×10‐6	1×10‐6	NUM
eurjchem-1635	201	26	,	,	PUNCT
eurjchem-1635	201	27	1×10‐5	1×10‐5	NUM
eurjchem-1635	201	28	,	,	PUNCT
eurjchem-1635	201	29	1×10‐4	1×10‐4	NUM
eurjchem-1635	201	30	and	and	CCONJ
eurjchem-1635	201	31	1×10‐3	1×10‐3	NUM
eurjchem-1635	201	32	m	m	NOUN
eurjchem-1635	201	33	of	of	ADP
eurjchem-1635	201	34	each	each	DET
eurjchem-1635	201	35	compound	compound	NOUN
eurjchem-1635	201	36	.	.	PUNCT
eurjchem-1635	202	1	following	follow	VERB
eurjchem-1635	202	2	this	this	PRON
eurjchem-1635	202	3	,	,	PUNCT
eurjchem-1635	202	4	cells	cell	NOUN
eurjchem-1635	202	5	were	be	AUX
eurjchem-1635	202	6	fixed	fix	VERB
eurjchem-1635	202	7	and	and	CCONJ
eurjchem-1635	202	8	stained	stain	VERB
eurjchem-1635	202	9	with	with	ADP
eurjchem-1635	202	10	protein	protein	NOUN
eurjchem-1635	202	11	binding	bind	VERB
eurjchem-1635	202	12	srb	srb	PROPN
eurjchem-1635	202	13	stain	stain	NOUN
eurjchem-1635	202	14	.	.	PUNCT
eurjchem-1635	203	1	excess	excess	ADJ
eurjchem-1635	203	2	stain	stain	NOUN
eurjchem-1635	203	3	is	be	AUX
eurjchem-1635	203	4	washed	wash	VERB
eurjchem-1635	203	5	and	and	CCONJ
eurjchem-1635	203	6	bound	bind	VERB
eurjchem-1635	203	7	stain	stain	NOUN
eurjchem-1635	203	8	was	be	AUX
eurjchem-1635	203	9	solubilized	solubilize	VERB
eurjchem-1635	203	10	,	,	PUNCT
eurjchem-1635	203	11	and	and	CCONJ
eurjchem-1635	203	12	the	the	DET
eurjchem-1635	203	13	absorbance	absorbance	NOUN
eurjchem-1635	203	14	was	be	AUX
eurjchem-1635	203	15	measured	measure	VERB
eurjchem-1635	203	16	at	at	ADP
eurjchem-1635	203	17	492	492	NUM
eurjchem-1635	203	18	nm	nm	NOUN
eurjchem-1635	203	19	in	in	ADP
eurjchem-1635	203	20	a	a	DET
eurjchem-1635	203	21	plate	plate	NOUN
eurjchem-1635	203	22	reader	reader	NOUN
eurjchem-1635	203	23	.	.	PUNCT
eurjchem-1635	204	1	concentration	concentration	NOUN
eurjchem-1635	204	2	of	of	ADP
eurjchem-1635	204	3	the	the	DET
eurjchem-1635	204	4	compounds	compound	NOUN
eurjchem-1635	204	5	that	that	PRON
eurjchem-1635	204	6	inhibited	inhibit	VERB
eurjchem-1635	204	7	50	50	NUM
eurjchem-1635	204	8	%	%	NOUN
eurjchem-1635	204	9	of	of	ADP
eurjchem-1635	204	10	the	the	DET
eurjchem-1635	204	11	net	net	ADJ
eurjchem-1635	204	12	cell	cell	NOUN
eurjchem-1635	204	13	growth	growth	NOUN
eurjchem-1635	204	14	,	,	PUNCT
eurjchem-1635	204	15	growth	growth	NOUN
eurjchem-1635	204	16	inhibition	inhibition	NOUN
eurjchem-1635	204	17	of	of	ADP
eurjchem-1635	204	18	50	50	NUM
eurjchem-1635	204	19	%	%	NOUN
eurjchem-1635	204	20	(	(	PUNCT
eurjchem-1635	204	21	gi50	gi50	PROPN
eurjchem-1635	204	22	)	)	PUNCT
eurjchem-1635	204	23	,	,	PUNCT
eurjchem-1635	204	24	was	be	AUX
eurjchem-1635	204	25	calculated	calculate	VERB
eurjchem-1635	204	26	from	from	ADP
eurjchem-1635	204	27	the	the	DET
eurjchem-1635	204	28	dose	dose	NOUN
eurjchem-1635	204	29	response	response	NOUN
eurjchem-1635	204	30	curve	curve	NOUN
eurjchem-1635	204	31	obtained	obtain	VERB
eurjchem-1635	204	32	for	for	ADP
eurjchem-1635	204	33	each	each	DET
eurjchem-1635	204	34	test	test	NOUN
eurjchem-1635	204	35	compound	compound	NOUN
eurjchem-1635	204	36	and	and	CCONJ
eurjchem-1635	204	37	cell	cell	NOUN
eurjchem-1635	204	38	line	line	NOUN
eurjchem-1635	204	39	.	.	PUNCT
eurjchem-1635	205	1	gi50	gi50	PROPN
eurjchem-1635	205	2	values	value	NOUN
eurjchem-1635	205	3	were	be	AUX
eurjchem-1635	205	4	presented	present	VERB
eurjchem-1635	205	5	in	in	ADP
eurjchem-1635	205	6	micro	micro	PROPN
eurjchem-1635	205	7	molar	molar	NOUN
eurjchem-1635	205	8	(	(	PUNCT
eurjchem-1635	205	9	μm	μm	NUM
eurjchem-1635	205	10	)	)	PUNCT
eurjchem-1635	205	11	concentration	concentration	NOUN
eurjchem-1635	205	12	.	.	PUNCT
eurjchem-1635	206	1	5‐flourouracil	5‐flourouracil	NUM
eurjchem-1635	206	2	(	(	PUNCT
eurjchem-1635	206	3	5‐fu	5‐fu	NUM
eurjchem-1635	206	4	)	)	PUNCT
eurjchem-1635	206	5	was	be	AUX
eurjchem-1635	206	6	used	use	VERB
eurjchem-1635	206	7	as	as	ADP
eurjchem-1635	206	8	positive	positive	ADJ
eurjchem-1635	206	9	control	control	NOUN
eurjchem-1635	206	10	for	for	ADP
eurjchem-1635	206	11	the	the	DET
eurjchem-1635	206	12	comparison	comparison	NOUN
eurjchem-1635	206	13	of	of	ADP
eurjchem-1635	206	14	cytotoxicity	cytotoxicity	NOUN
eurjchem-1635	206	15	of	of	ADP
eurjchem-1635	206	16	synthesized	synthesize	VERB
eurjchem-1635	206	17	compounds	compound	NOUN
eurjchem-1635	206	18	.	.	PUNCT
eurjchem-1635	207	1	assays	assay	NOUN
eurjchem-1635	207	2	were	be	AUX
eurjchem-1635	207	3	performed	perform	VERB
eurjchem-1635	207	4	in	in	ADP
eurjchem-1635	207	5	triplicate	triplicate	NOUN
eurjchem-1635	207	6	on	on	ADP
eurjchem-1635	207	7	three	three	NUM
eurjchem-1635	207	8	independent	independent	ADJ
eurjchem-1635	207	9	experiments	experiment	NOUN
eurjchem-1635	207	10	and	and	CCONJ
eurjchem-1635	207	11	their	their	PRON
eurjchem-1635	207	12	mean	mean	ADJ
eurjchem-1635	207	13	values	value	NOUN
eurjchem-1635	207	14	are	be	AUX
eurjchem-1635	207	15	taken	take	VERB
eurjchem-1635	207	16	as	as	ADP
eurjchem-1635	207	17	a	a	DET
eurjchem-1635	207	18	final	final	ADJ
eurjchem-1635	207	19	reading	reading	NOUN
eurjchem-1635	207	20	.	.	PUNCT
eurjchem-1635	208	1	all	all	DET
eurjchem-1635	208	2	experiments	experiment	NOUN
eurjchem-1635	208	3	were	be	AUX
eurjchem-1635	208	4	performed	perform	VERB
eurjchem-1635	208	5	in	in	ADP
eurjchem-1635	208	6	duplicate	duplicate	NOUN
eurjchem-1635	208	7	and	and	CCONJ
eurjchem-1635	208	8	repeated	repeat	VERB
eurjchem-1635	208	9	three	three	NUM
eurjchem-1635	208	10	times	time	NOUN
eurjchem-1635	208	11	.	.	PUNCT
eurjchem-1635	209	1	388	388	NUM
eurjchem-1635	209	2	pawar	pawar	PROPN
eurjchem-1635	209	3	et	et	PROPN
eurjchem-1635	209	4	al	al	PROPN
eurjchem-1635	209	5	.	.	PUNCT
eurjchem-1635	209	6	/	/	SYM
eurjchem-1635	209	7	european	european	PROPN
eurjchem-1635	209	8	journal	journal	PROPN
eurjchem-1635	209	9	of	of	ADP
eurjchem-1635	209	10	chemistry	chemistry	NOUN
eurjchem-1635	209	11	8	8	NUM
eurjchem-1635	209	12	(	(	PUNCT
eurjchem-1635	209	13	4	4	NUM
eurjchem-1635	209	14	)	)	PUNCT
eurjchem-1635	209	15	(	(	PUNCT
eurjchem-1635	209	16	2017	2017	NUM
eurjchem-1635	209	17	)	)	PUNCT
eurjchem-1635	209	18	384‐390	384‐390	NUM
eurjchem-1635	209	19	table	table	NOUN
eurjchem-1635	209	20	1	1	NUM
eurjchem-1635	209	21	.	.	PUNCT
eurjchem-1635	209	22	screening	screen	VERB
eurjchem-1635	209	23	conditions	condition	NOUN
eurjchem-1635	209	24	for	for	ADP
eurjchem-1635	209	25	step	step	NOUN
eurjchem-1635	209	26	(	(	PUNCT
eurjchem-1635	209	27	a	a	NOUN
eurjchem-1635	209	28	)	)	PUNCT
eurjchem-1635	209	29	in	in	ADP
eurjchem-1635	209	30	scheme	scheme	NOUN
eurjchem-1635	209	31	1	1	NUM
eurjchem-1635	209	32	and	and	CCONJ
eurjchem-1635	209	33	2	2	NUM
eurjchem-1635	209	34	.	.	NOUN
eurjchem-1635	209	35	entry	entry	NOUN
eurjchem-1635	209	36	base	base	NOUN
eurjchem-1635	209	37	(	(	PUNCT
eurjchem-1635	209	38	3	3	NUM
eurjchem-1635	209	39	equiv	equiv	NOUN
eurjchem-1635	209	40	.	.	PUNCT
eurjchem-1635	209	41	)	)	PUNCT
eurjchem-1635	210	1	solvent	solvent	ADJ
eurjchem-1635	210	2	temperature	temperature	NOUN
eurjchem-1635	210	3	(	(	PUNCT
eurjchem-1635	210	4	°	°	ADP
eurjchem-1635	210	5	c	c	NOUN
eurjchem-1635	210	6	)	)	PUNCT
eurjchem-1635	210	7	time	time	NOUN
eurjchem-1635	210	8	(	(	PUNCT
eurjchem-1635	210	9	h	h	NOUN
eurjchem-1635	210	10	)	)	PUNCT
eurjchem-1635	210	11	yield	yield	NOUN
eurjchem-1635	210	12	(	(	PUNCT
eurjchem-1635	210	13	%	%	INTJ
eurjchem-1635	210	14	)	)	PUNCT
eurjchem-1635	210	15	a	a	PRON
eurjchem-1635	210	16	,	,	PUNCT
eurjchem-1635	210	17	compound	compound	NOUN
eurjchem-1635	210	18	1	1	NUM
eurjchem-1635	210	19	and	and	CCONJ
eurjchem-1635	210	20	1a	1a	NUM
eurjchem-1635	210	21	1	1	NUM
eurjchem-1635	210	22	k2co3	k2co3	ADJ
eurjchem-1635	210	23	acetone	acetone	NOUN
eurjchem-1635	210	24	70	70	NUM
eurjchem-1635	210	25	12	12	NUM
eurjchem-1635	210	26	35	35	NUM
eurjchem-1635	210	27	,	,	PUNCT
eurjchem-1635	210	28	25	25	NUM
eurjchem-1635	210	29	2	2	NUM
eurjchem-1635	210	30	k2co3	k2co3	ADJ
eurjchem-1635	210	31	dmf	dmf	PROPN
eurjchem-1635	210	32	110	110	NUM
eurjchem-1635	210	33	12	12	NUM
eurjchem-1635	210	34	25	25	NUM
eurjchem-1635	210	35	,	,	PUNCT
eurjchem-1635	210	36	32	32	NUM
eurjchem-1635	210	37	3	3	NUM
eurjchem-1635	210	38	k2co3	k2co3	ADJ
eurjchem-1635	210	39	toluene	toluene	NOUN
eurjchem-1635	210	40	100	100	NUM
eurjchem-1635	210	41	12	12	NUM
eurjchem-1635	210	42	40	40	NUM
eurjchem-1635	210	43	,	,	PUNCT
eurjchem-1635	210	44	36	36	NUM
eurjchem-1635	210	45	4	4	NUM
eurjchem-1635	210	46	cs2co3	cs2co3	VERB
eurjchem-1635	210	47	acetone	acetone	NOUN
eurjchem-1635	210	48	70	70	NUM
eurjchem-1635	210	49	12	12	NUM
eurjchem-1635	210	50	45	45	NUM
eurjchem-1635	210	51	,	,	PUNCT
eurjchem-1635	210	52	25	25	NUM
eurjchem-1635	210	53	5	5	NUM
eurjchem-1635	210	54	cs2co3	cs2co3	VERB
eurjchem-1635	210	55	dmf	dmf	NOUN
eurjchem-1635	210	56	110	110	NUM
eurjchem-1635	210	57	12	12	NUM
eurjchem-1635	210	58	40	40	NUM
eurjchem-1635	210	59	,	,	PUNCT
eurjchem-1635	210	60	29	29	NUM
eurjchem-1635	210	61	6	6	NUM
eurjchem-1635	210	62	cs2co3	cs2co3	VERB
eurjchem-1635	210	63	toluene	toluene	NOUN
eurjchem-1635	210	64	110	110	NUM
eurjchem-1635	210	65	12	12	NUM
eurjchem-1635	210	66	70	70	NUM
eurjchem-1635	210	67	,	,	PUNCT
eurjchem-1635	210	68	10	10	NUM
eurjchem-1635	210	69	7	7	NUM
eurjchem-1635	210	70	kotbu	kotbu	PROPN
eurjchem-1635	210	71	dmf	dmf	PROPN
eurjchem-1635	210	72	110	110	NUM
eurjchem-1635	210	73	12	12	NUM
eurjchem-1635	210	74	37	37	NUM
eurjchem-1635	210	75	,	,	PUNCT
eurjchem-1635	210	76	25	25	NUM
eurjchem-1635	210	77	8	8	NUM
eurjchem-1635	210	78	kotbu	kotbu	NOUN
eurjchem-1635	210	79	toluene	toluene	NOUN
eurjchem-1635	210	80	110	110	NUM
eurjchem-1635	210	81	12	12	NUM
eurjchem-1635	210	82	35	35	NUM
eurjchem-1635	210	83	,	,	PUNCT
eurjchem-1635	210	84	38	38	NUM
eurjchem-1635	210	85	9	9	NUM
eurjchem-1635	210	86	na2co3	na2co3	PROPN
eurjchem-1635	210	87	dmf	dmf	PROPN
eurjchem-1635	210	88	110	110	NUM
eurjchem-1635	210	89	12	12	NUM
eurjchem-1635	210	90	20	20	NUM
eurjchem-1635	210	91	,	,	PUNCT
eurjchem-1635	210	92	45	45	NUM
eurjchem-1635	210	93	10	10	NUM
eurjchem-1635	210	94	na2co3	na2co3	ADJ
eurjchem-1635	210	95	toluene	toluene	NOUN
eurjchem-1635	210	96	110	110	NUM
eurjchem-1635	210	97	12	12	NUM
eurjchem-1635	210	98	25	25	NUM
eurjchem-1635	210	99	,	,	PUNCT
eurjchem-1635	210	100	51	51	NUM
eurjchem-1635	210	101	11	11	NUM
eurjchem-1635	210	102	k3po4	k3po4	NOUN
eurjchem-1635	210	103	dmf	dmf	PROPN
eurjchem-1635	210	104	110	110	NUM
eurjchem-1635	210	105	12	12	NUM
eurjchem-1635	210	106	45	45	NUM
eurjchem-1635	210	107	,	,	PUNCT
eurjchem-1635	210	108	30	30	NUM
eurjchem-1635	210	109	12	12	NUM
eurjchem-1635	210	110	k3po4	k3po4	NOUN
eurjchem-1635	210	111	toluene	toluene	NOUN
eurjchem-1635	210	112	110	110	NUM
eurjchem-1635	210	113	12	12	NUM
eurjchem-1635	210	114	35	35	NUM
eurjchem-1635	210	115	,	,	PUNCT
eurjchem-1635	210	116	31	31	NUM
eurjchem-1635	210	117	a	a	DET
eurjchem-1635	210	118	isolated	isolated	ADJ
eurjchem-1635	210	119	yield	yield	NOUN
eurjchem-1635	210	120	.	.	PUNCT
eurjchem-1635	211	1	the	the	DET
eurjchem-1635	211	2	1h	1h	NUM
eurjchem-1635	211	3	nmr	nmr	NOUN
eurjchem-1635	211	4	of	of	ADP
eurjchem-1635	211	5	compound	compound	NOUN
eurjchem-1635	211	6	1	1	NUM
eurjchem-1635	211	7	shows	show	VERB
eurjchem-1635	211	8	protons	proton	NOUN
eurjchem-1635	211	9	at	at	ADP
eurjchem-1635	211	10	3.42	3.42	NUM
eurjchem-1635	211	11	(	(	PUNCT
eurjchem-1635	211	12	dd	dd	PROPN
eurjchem-1635	211	13	,	,	PUNCT
eurjchem-1635	211	14	1h	1h	NUM
eurjchem-1635	211	15	,	,	PUNCT
eurjchem-1635	211	16	j	j	PROPN
eurjchem-1635	211	17	=	=	PROPN
eurjchem-1635	211	18	12.8	12.8	NUM
eurjchem-1635	211	19	,	,	PUNCT
eurjchem-1635	211	20	3.8	3.8	NUM
eurjchem-1635	211	21	hz	hz	NOUN
eurjchem-1635	211	22	,	,	PUNCT
eurjchem-1635	211	23	nh‐ch2	nh‐ch2	ADJ
eurjchem-1635	211	24	)	)	PUNCT
eurjchem-1635	211	25	,	,	PUNCT
eurjchem-1635	211	26	3.58	3.58	NUM
eurjchem-1635	211	27	(	(	PUNCT
eurjchem-1635	211	28	dd	dd	PROPN
eurjchem-1635	211	29	,	,	PUNCT
eurjchem-1635	211	30	1h	1h	NUM
eurjchem-1635	211	31	,	,	PUNCT
eurjchem-1635	211	32	j	j	PROPN
eurjchem-1635	211	33	=	=	PROPN
eurjchem-1635	211	34	12.4	12.4	NUM
eurjchem-1635	211	35	,	,	PUNCT
eurjchem-1635	211	36	3.6	3.6	NUM
eurjchem-1635	211	37	hz	hz	NOUN
eurjchem-1635	211	38	,	,	PUNCT
eurjchem-1635	211	39	nh‐ch2	nh‐ch2	ADJ
eurjchem-1635	211	40	)	)	PUNCT
eurjchem-1635	211	41	,	,	PUNCT
eurjchem-1635	211	42	5.57	5.57	NUM
eurjchem-1635	211	43	(	(	PUNCT
eurjchem-1635	211	44	s	s	PROPN
eurjchem-1635	211	45	,	,	PUNCT
eurjchem-1635	211	46	1h	1h	NUM
eurjchem-1635	211	47	,	,	PUNCT
eurjchem-1635	211	48	cn‐ch	cn‐ch	NUM
eurjchem-1635	211	49	)	)	PUNCT
eurjchem-1635	211	50	,	,	PUNCT
eurjchem-1635	211	51	6.19	6.19	NUM
eurjchem-1635	211	52	(	(	PUNCT
eurjchem-1635	211	53	s	s	PROPN
eurjchem-1635	211	54	,	,	PUNCT
eurjchem-1635	211	55	1h	1h	NUM
eurjchem-1635	211	56	,	,	PUNCT
eurjchem-1635	211	57	nh	nh	PROPN
eurjchem-1635	211	58	)	)	PUNCT
eurjchem-1635	211	59	,	,	PUNCT
eurjchem-1635	211	60	6.58	6.58	NUM
eurjchem-1635	211	61	(	(	PUNCT
eurjchem-1635	211	62	q	q	NOUN
eurjchem-1635	211	63	,	,	PUNCT
eurjchem-1635	211	64	1h	1h	NUM
eurjchem-1635	211	65	,	,	PUNCT
eurjchem-1635	211	66	ar‐h	ar‐h	NOUN
eurjchem-1635	211	67	)	)	PUNCT
eurjchem-1635	211	68	,	,	PUNCT
eurjchem-1635	211	69	6.64	6.64	NUM
eurjchem-1635	211	70	(	(	PUNCT
eurjchem-1635	211	71	d	d	PROPN
eurjchem-1635	211	72	,	,	PUNCT
eurjchem-1635	211	73	1h	1h	NUM
eurjchem-1635	211	74	,	,	PUNCT
eurjchem-1635	211	75	j	j	PROPN
eurjchem-1635	211	76	=	=	PROPN
eurjchem-1635	211	77	8.82	8.82	NUM
eurjchem-1635	211	78	hz	hz	NOUN
eurjchem-1635	211	79	,	,	PUNCT
eurjchem-1635	211	80	ar‐h	ar‐h	PROPN
eurjchem-1635	211	81	)	)	PUNCT
eurjchem-1635	211	82	,	,	PUNCT
eurjchem-1635	211	83	6.78	6.78	NUM
eurjchem-1635	211	84	(	(	PUNCT
eurjchem-1635	211	85	q	q	NOUN
eurjchem-1635	211	86	,	,	PUNCT
eurjchem-1635	211	87	2h	2h	NUM
eurjchem-1635	211	88	,	,	PUNCT
eurjchem-1635	211	89	ar‐h	ar‐h	NOUN
eurjchem-1635	211	90	)	)	PUNCT
eurjchem-1635	211	91	.	.	PUNCT
eurjchem-1635	212	1	scheme	scheme	NOUN
eurjchem-1635	212	2	3	3	NUM
eurjchem-1635	212	3	3	3	NUM
eurjchem-1635	212	4	.	.	PUNCT
eurjchem-1635	212	5	results	result	NOUN
eurjchem-1635	212	6	and	and	CCONJ
eurjchem-1635	212	7	discussion	discussion	NOUN
eurjchem-1635	212	8	3.1	3.1	NUM
eurjchem-1635	212	9	.	.	PUNCT
eurjchem-1635	213	1	synthesis	synthesis	VERB
eurjchem-1635	213	2	the	the	DET
eurjchem-1635	213	3	synthetic	synthetic	ADJ
eurjchem-1635	213	4	methods	method	NOUN
eurjchem-1635	213	5	adopted	adopt	VERB
eurjchem-1635	213	6	for	for	ADP
eurjchem-1635	213	7	the	the	DET
eurjchem-1635	213	8	preparation	preparation	NOUN
eurjchem-1635	213	9	of	of	ADP
eurjchem-1635	213	10	the	the	DET
eurjchem-1635	213	11	title	title	NOUN
eurjchem-1635	213	12	compounds	compound	VERB
eurjchem-1635	213	13	4a‐e	4a‐e	NOUN
eurjchem-1635	213	14	and	and	CCONJ
eurjchem-1635	213	15	7a‐e	7a‐e	PROPN
eurjchem-1635	213	16	is	be	AUX
eurjchem-1635	213	17	depicted	depict	VERB
eurjchem-1635	213	18	in	in	ADP
eurjchem-1635	213	19	the	the	DET
eurjchem-1635	213	20	scheme	scheme	NOUN
eurjchem-1635	213	21	1	1	NUM
eurjchem-1635	213	22	and	and	CCONJ
eurjchem-1635	213	23	2	2	NUM
eurjchem-1635	213	24	presented	present	VERB
eurjchem-1635	213	25	below	below	ADV
eurjchem-1635	213	26	.	.	PUNCT
eurjchem-1635	214	1	an	an	DET
eurjchem-1635	214	2	initial	initial	ADJ
eurjchem-1635	214	3	investigation	investigation	NOUN
eurjchem-1635	214	4	of	of	ADP
eurjchem-1635	214	5	reaction	reaction	NOUN
eurjchem-1635	214	6	conditions	condition	NOUN
eurjchem-1635	214	7	for	for	ADP
eurjchem-1635	214	8	step	step	NOUN
eurjchem-1635	214	9	(	(	PUNCT
eurjchem-1635	214	10	a	a	NOUN
eurjchem-1635	214	11	)	)	PUNCT
eurjchem-1635	214	12	was	be	AUX
eurjchem-1635	214	13	done	do	VERB
eurjchem-1635	214	14	by	by	ADP
eurjchem-1635	214	15	using	use	VERB
eurjchem-1635	214	16	2‐aminophenol	2‐aminophenol	NUM
eurjchem-1635	214	17	(	(	PUNCT
eurjchem-1635	214	18	1	1	NUM
eurjchem-1635	214	19	equiv	equiv	NOUN
eurjchem-1635	214	20	.	.	PUNCT
eurjchem-1635	214	21	)	)	PUNCT
eurjchem-1635	215	1	react	react	VERB
eurjchem-1635	215	2	with	with	ADP
eurjchem-1635	215	3	2‐chloroacrylonitrile	2‐chloroacrylonitrile	ADJ
eurjchem-1635	215	4	(	(	PUNCT
eurjchem-1635	215	5	1.2	1.2	NUM
eurjchem-1635	215	6	equiv	equiv	NOUN
eurjchem-1635	215	7	.	.	PUNCT
eurjchem-1635	215	8	)	)	PUNCT
eurjchem-1635	216	1	and	and	CCONJ
eurjchem-1635	216	2	2‐	2‐	NUM
eurjchem-1635	216	3	chloromethylacrylonitrile	chloromethylacrylonitrile	NOUN
eurjchem-1635	216	4	(	(	PUNCT
eurjchem-1635	216	5	1.2	1.2	NUM
eurjchem-1635	216	6	equiv	equiv	NOUN
eurjchem-1635	216	7	.	.	PUNCT
eurjchem-1635	216	8	)	)	PUNCT
eurjchem-1635	216	9	by	by	ADP
eurjchem-1635	216	10	using	use	VERB
eurjchem-1635	216	11	different	different	ADJ
eurjchem-1635	216	12	bases	basis	NOUN
eurjchem-1635	216	13	,	,	PUNCT
eurjchem-1635	216	14	solvents	solvent	NOUN
eurjchem-1635	216	15	and	and	CCONJ
eurjchem-1635	216	16	temperature	temperature	NOUN
eurjchem-1635	216	17	.	.	PUNCT
eurjchem-1635	217	1	the	the	DET
eurjchem-1635	217	2	results	result	NOUN
eurjchem-1635	217	3	are	be	AUX
eurjchem-1635	217	4	tabulated	tabulate	VERB
eurjchem-1635	217	5	in	in	ADP
eurjchem-1635	217	6	table	table	NOUN
eurjchem-1635	217	7	1	1	NUM
eurjchem-1635	217	8	.	.	PUNCT
eurjchem-1635	218	1	we	we	PRON
eurjchem-1635	218	2	have	have	AUX
eurjchem-1635	218	3	screened	screen	VERB
eurjchem-1635	218	4	k2co3	k2co3	ADJ
eurjchem-1635	218	5	in	in	ADP
eurjchem-1635	218	6	entry	entry	NOUN
eurjchem-1635	218	7	1	1	NUM
eurjchem-1635	218	8	,	,	PUNCT
eurjchem-1635	218	9	2	2	NUM
eurjchem-1635	218	10	and	and	CCONJ
eurjchem-1635	218	11	3	3	NUM
eurjchem-1635	218	12	by	by	ADP
eurjchem-1635	218	13	taking	take	VERB
eurjchem-1635	218	14	solvents	solvent	NOUN
eurjchem-1635	218	15	acetone	acetone	NOUN
eurjchem-1635	218	16	dmf	dmf	PROPN
eurjchem-1635	218	17	and	and	CCONJ
eurjchem-1635	218	18	toluene	toluene	NOUN
eurjchem-1635	218	19	for	for	ADP
eurjchem-1635	218	20	70	70	NUM
eurjchem-1635	218	21	,	,	PUNCT
eurjchem-1635	218	22	110	110	NUM
eurjchem-1635	218	23	and	and	CCONJ
eurjchem-1635	218	24	100	100	NUM
eurjchem-1635	218	25	°	°	NOUN
eurjchem-1635	218	26	c	c	NOUN
eurjchem-1635	218	27	,	,	PUNCT
eurjchem-1635	218	28	respectively	respectively	ADV
eurjchem-1635	218	29	for	for	ADP
eurjchem-1635	218	30	12	12	NUM
eurjchem-1635	218	31	h	h	NOUN
eurjchem-1635	218	32	(	(	PUNCT
eurjchem-1635	218	33	for	for	ADP
eurjchem-1635	218	34	entry	entry	NOUN
eurjchem-1635	218	35	1	1	NUM
eurjchem-1635	218	36	and	and	CCONJ
eurjchem-1635	218	37	4	4	NUM
eurjchem-1635	218	38	,	,	PUNCT
eurjchem-1635	218	39	we	we	PRON
eurjchem-1635	218	40	have	have	AUX
eurjchem-1635	218	41	used	use	VERB
eurjchem-1635	218	42	chilled	chill	VERB
eurjchem-1635	218	43	water	water	NOUN
eurjchem-1635	218	44	circulation	circulation	NOUN
eurjchem-1635	218	45	)	)	PUNCT
eurjchem-1635	218	46	.	.	PUNCT
eurjchem-1635	219	1	after	after	ADP
eurjchem-1635	219	2	column	column	NOUN
eurjchem-1635	219	3	purification	purification	NOUN
eurjchem-1635	219	4	,	,	PUNCT
eurjchem-1635	219	5	we	we	PRON
eurjchem-1635	219	6	have	have	AUX
eurjchem-1635	219	7	obtained	obtain	VERB
eurjchem-1635	219	8	desired	desire	VERB
eurjchem-1635	219	9	product	product	NOUN
eurjchem-1635	219	10	in	in	ADP
eurjchem-1635	219	11	35	35	NUM
eurjchem-1635	219	12	,	,	PUNCT
eurjchem-1635	219	13	25	25	NUM
eurjchem-1635	219	14	and	and	CCONJ
eurjchem-1635	219	15	40	40	NUM
eurjchem-1635	219	16	%	%	NOUN
eurjchem-1635	219	17	,	,	PUNCT
eurjchem-1635	219	18	respectively	respectively	ADV
eurjchem-1635	219	19	.	.	PUNCT
eurjchem-1635	220	1	in	in	ADP
eurjchem-1635	220	2	entry	entry	NOUN
eurjchem-1635	220	3	4	4	NUM
eurjchem-1635	220	4	,	,	PUNCT
eurjchem-1635	220	5	5	5	NUM
eurjchem-1635	220	6	and	and	CCONJ
eurjchem-1635	220	7	6	6	NUM
eurjchem-1635	220	8	,	,	PUNCT
eurjchem-1635	220	9	we	we	PRON
eurjchem-1635	220	10	have	have	AUX
eurjchem-1635	220	11	used	use	VERB
eurjchem-1635	220	12	cs2co3	cs2co3	VERB
eurjchem-1635	220	13	in	in	ADP
eurjchem-1635	220	14	acetone	acetone	NOUN
eurjchem-1635	220	15	dmf	dmf	PROPN
eurjchem-1635	220	16	and	and	CCONJ
eurjchem-1635	220	17	toluene	toluene	NOUN
eurjchem-1635	220	18	to	to	PART
eurjchem-1635	220	19	obtain	obtain	VERB
eurjchem-1635	220	20	yields	yield	NOUN
eurjchem-1635	220	21	from	from	ADP
eurjchem-1635	220	22	45	45	NUM
eurjchem-1635	220	23	,	,	PUNCT
eurjchem-1635	220	24	40	40	NUM
eurjchem-1635	220	25	and	and	CCONJ
eurjchem-1635	220	26	70	70	NUM
eurjchem-1635	220	27	%	%	NOUN
eurjchem-1635	220	28	,	,	PUNCT
eurjchem-1635	220	29	respectively	respectively	ADV
eurjchem-1635	220	30	.	.	PUNCT
eurjchem-1635	221	1	in	in	ADP
eurjchem-1635	221	2	conditions	condition	NOUN
eurjchem-1635	221	3	7	7	NUM
eurjchem-1635	221	4	to	to	PART
eurjchem-1635	221	5	12	12	NUM
eurjchem-1635	221	6	,	,	PUNCT
eurjchem-1635	221	7	we	we	PRON
eurjchem-1635	221	8	have	have	AUX
eurjchem-1635	221	9	used	use	VERB
eurjchem-1635	221	10	potassium	potassium	NOUN
eurjchem-1635	221	11	tert	tert	NOUN
eurjchem-1635	221	12	butoxide	butoxide	NOUN
eurjchem-1635	221	13	(	(	PUNCT
eurjchem-1635	221	14	kotbu	kotbu	PROPN
eurjchem-1635	221	15	)	)	PUNCT
eurjchem-1635	221	16	,	,	PUNCT
eurjchem-1635	221	17	na2co3	na2co3	NOUN
eurjchem-1635	221	18	and	and	CCONJ
eurjchem-1635	221	19	k3po4	k3po4	NOUN
eurjchem-1635	221	20	in	in	ADP
eurjchem-1635	221	21	dmf	dmf	PROPN
eurjchem-1635	221	22	and	and	CCONJ
eurjchem-1635	221	23	toluene	toluene	NOUN
eurjchem-1635	221	24	as	as	ADP
eurjchem-1635	221	25	solvents	solvent	NOUN
eurjchem-1635	221	26	the	the	DET
eurjchem-1635	221	27	yields	yield	NOUN
eurjchem-1635	221	28	are	be	AUX
eurjchem-1635	221	29	in	in	ADP
eurjchem-1635	221	30	the	the	DET
eurjchem-1635	221	31	range	range	NOUN
eurjchem-1635	221	32	of	of	ADP
eurjchem-1635	221	33	20	20	NUM
eurjchem-1635	221	34	to	to	PART
eurjchem-1635	221	35	45	45	NUM
eurjchem-1635	221	36	%	%	NOUN
eurjchem-1635	221	37	.	.	PUNCT
eurjchem-1635	222	1	with	with	ADP
eurjchem-1635	222	2	k3po4	k3po4	VERB
eurjchem-1635	222	3	the	the	DET
eurjchem-1635	222	4	yield	yield	NOUN
eurjchem-1635	222	5	of	of	ADP
eurjchem-1635	222	6	compound	compound	NOUN
eurjchem-1635	222	7	1	1	NUM
eurjchem-1635	222	8	and	and	CCONJ
eurjchem-1635	222	9	1a	1a	X
eurjchem-1635	222	10	is	be	AUX
eurjchem-1635	222	11	like	like	ADP
eurjchem-1635	222	12	60	60	NUM
eurjchem-1635	222	13	to	to	PART
eurjchem-1635	222	14	40	40	NUM
eurjchem-1635	222	15	%	%	NOUN
eurjchem-1635	222	16	,	,	PUNCT
eurjchem-1635	222	17	respectively	respectively	ADV
eurjchem-1635	222	18	,	,	PUNCT
eurjchem-1635	222	19	so	so	ADV
eurjchem-1635	222	20	,	,	PUNCT
eurjchem-1635	222	21	it	it	PRON
eurjchem-1635	222	22	is	be	AUX
eurjchem-1635	222	23	not	not	PART
eurjchem-1635	222	24	favorable	favorable	ADJ
eurjchem-1635	222	25	and	and	CCONJ
eurjchem-1635	222	26	that	that	PRON
eurjchem-1635	222	27	of	of	ADP
eurjchem-1635	222	28	na2co3	na2co3	PROPN
eurjchem-1635	222	29	the	the	DET
eurjchem-1635	222	30	undesired	undesired	ADJ
eurjchem-1635	222	31	compound	compound	NOUN
eurjchem-1635	222	32	1a	1a	PROPN
eurjchem-1635	222	33	is	be	AUX
eurjchem-1635	222	34	major	major	ADJ
eurjchem-1635	222	35	isolated	isolated	ADJ
eurjchem-1635	222	36	compound	compound	NOUN
eurjchem-1635	222	37	compared	compare	VERB
eurjchem-1635	222	38	to	to	ADP
eurjchem-1635	222	39	desired	desire	VERB
eurjchem-1635	222	40	isolated	isolated	ADJ
eurjchem-1635	222	41	compound	compound	NOUN
eurjchem-1635	222	42	1	1	NUM
eurjchem-1635	222	43	,	,	PUNCT
eurjchem-1635	222	44	confirmed	confirm	VERB
eurjchem-1635	222	45	from	from	ADP
eurjchem-1635	222	46	entries	entry	NOUN
eurjchem-1635	222	47	9	9	NUM
eurjchem-1635	222	48	to	to	PART
eurjchem-1635	222	49	12	12	NUM
eurjchem-1635	222	50	.	.	PUNCT
eurjchem-1635	223	1	in	in	ADP
eurjchem-1635	223	2	all	all	DET
eurjchem-1635	223	3	conditions	condition	NOUN
eurjchem-1635	223	4	,	,	PUNCT
eurjchem-1635	223	5	there	there	PRON
eurjchem-1635	223	6	is	be	VERB
eurjchem-1635	223	7	formation	formation	NOUN
eurjchem-1635	223	8	of	of	ADP
eurjchem-1635	223	9	two	two	NUM
eurjchem-1635	223	10	merged	merge	VERB
eurjchem-1635	223	11	spots	spot	NOUN
eurjchem-1635	223	12	among	among	ADP
eurjchem-1635	223	13	them	they	PRON
eurjchem-1635	223	14	one	one	NUM
eurjchem-1635	223	15	is	be	AUX
eurjchem-1635	223	16	product	product	NOUN
eurjchem-1635	223	17	and	and	CCONJ
eurjchem-1635	223	18	one	one	NOUN
eurjchem-1635	223	19	is	be	AUX
eurjchem-1635	223	20	side	side	NOUN
eurjchem-1635	223	21	product	product	NOUN
eurjchem-1635	223	22	which	which	PRON
eurjchem-1635	223	23	is	be	AUX
eurjchem-1635	223	24	confirmed	confirm	VERB
eurjchem-1635	223	25	by	by	ADP
eurjchem-1635	223	26	separating	separate	VERB
eurjchem-1635	223	27	them	they	PRON
eurjchem-1635	223	28	.	.	PUNCT
eurjchem-1635	224	1	both	both	DET
eurjchem-1635	224	2	compounds	compound	NOUN
eurjchem-1635	224	3	are	be	AUX
eurjchem-1635	224	4	eluting	elute	VERB
eurjchem-1635	224	5	at	at	ADP
eurjchem-1635	224	6	same	same	ADJ
eurjchem-1635	224	7	polarity	polarity	NOUN
eurjchem-1635	224	8	of	of	ADP
eurjchem-1635	224	9	etoac	etoac	ADJ
eurjchem-1635	224	10	:	:	PUNCT
eurjchem-1635	224	11	hexane	hexane	NOUN
eurjchem-1635	224	12	(	(	PUNCT
eurjchem-1635	224	13	10:90	10:90	NUM
eurjchem-1635	224	14	,	,	PUNCT
eurjchem-1635	224	15	v	v	NOUN
eurjchem-1635	224	16	:	:	PUNCT
eurjchem-1635	224	17	v	v	NOUN
eurjchem-1635	224	18	)	)	PUNCT
eurjchem-1635	224	19	from	from	ADP
eurjchem-1635	224	20	column	column	NOUN
eurjchem-1635	224	21	chromatography	chromatography	NOUN
eurjchem-1635	224	22	.	.	PUNCT
eurjchem-1635	225	1	we	we	PRON
eurjchem-1635	225	2	have	have	AUX
eurjchem-1635	225	3	isolated	isolate	VERB
eurjchem-1635	225	4	both	both	DET
eurjchem-1635	225	5	compounds	compound	NOUN
eurjchem-1635	225	6	by	by	ADP
eurjchem-1635	225	7	column	column	NOUN
eurjchem-1635	225	8	chromatography	chromatography	NOUN
eurjchem-1635	225	9	by	by	ADP
eurjchem-1635	225	10	using	use	VERB
eurjchem-1635	225	11	silica	silica	NOUN
eurjchem-1635	225	12	gel	gel	NOUN
eurjchem-1635	225	13	(	(	PUNCT
eurjchem-1635	225	14	100‐200	100‐200	NUM
eurjchem-1635	225	15	mesh	mesh	NOUN
eurjchem-1635	225	16	)	)	PUNCT
eurjchem-1635	225	17	and	and	CCONJ
eurjchem-1635	225	18	confirmed	confirm	VERB
eurjchem-1635	225	19	the	the	DET
eurjchem-1635	225	20	structure	structure	NOUN
eurjchem-1635	225	21	of	of	ADP
eurjchem-1635	225	22	compound	compound	NOUN
eurjchem-1635	225	23	1	1	NUM
eurjchem-1635	225	24	by	by	ADP
eurjchem-1635	225	25	the	the	DET
eurjchem-1635	225	26	help	help	NOUN
eurjchem-1635	225	27	of	of	ADP
eurjchem-1635	225	28	nuclear	nuclear	ADJ
eurjchem-1635	225	29	overhauser	overhauser	NOUN
eurjchem-1635	225	30	effect	effect	NOUN
eurjchem-1635	225	31	(	(	PUNCT
eurjchem-1635	225	32	noe	noe	NOUN
eurjchem-1635	225	33	)	)	PUNCT
eurjchem-1635	225	34	experiments	experiment	NOUN
eurjchem-1635	225	35	there	there	PRON
eurjchem-1635	225	36	results	result	NOUN
eurjchem-1635	225	37	are	be	AUX
eurjchem-1635	225	38	depicted	depict	VERB
eurjchem-1635	225	39	in	in	ADP
eurjchem-1635	225	40	scheme	scheme	NOUN
eurjchem-1635	225	41	3	3	NUM
eurjchem-1635	225	42	.	.	PUNCT
eurjchem-1635	225	43	from	from	ADP
eurjchem-1635	225	44	first	first	ADJ
eurjchem-1635	225	45	noe	noe	PROPN
eurjchem-1635	225	46	experiment	experiment	NOUN
eurjchem-1635	225	47	on	on	ADP
eurjchem-1635	225	48	compound	compound	NOUN
eurjchem-1635	225	49	1	1	NUM
eurjchem-1635	225	50	,	,	PUNCT
eurjchem-1635	225	51	we	we	PRON
eurjchem-1635	225	52	have	have	AUX
eurjchem-1635	225	53	irradiated	irradiate	VERB
eurjchem-1635	225	54	proton	proton	NOUN
eurjchem-1635	225	55	at	at	ADP
eurjchem-1635	225	56	δ	δ	PROPN
eurjchem-1635	225	57	5.57	5.57	NUM
eurjchem-1635	225	58	ppm	ppm	NOUN
eurjchem-1635	225	59	,	,	PUNCT
eurjchem-1635	225	60	both	both	CCONJ
eurjchem-1635	225	61	the	the	DET
eurjchem-1635	225	62	protons	proton	NOUN
eurjchem-1635	225	63	of	of	ADP
eurjchem-1635	225	64	nh‐ch2	nh‐ch2	PROPN
eurjchem-1635	225	65	shows	show	VERB
eurjchem-1635	225	66	signals	signal	NOUN
eurjchem-1635	225	67	at	at	ADP
eurjchem-1635	225	68	δ	δ	PROPN
eurjchem-1635	225	69	3.58	3.58	NUM
eurjchem-1635	225	70	(	(	PUNCT
eurjchem-1635	225	71	weak	weak	ADJ
eurjchem-1635	225	72	)	)	PUNCT
eurjchem-1635	225	73	and	and	CCONJ
eurjchem-1635	225	74	3.42	3.42	NUM
eurjchem-1635	225	75	ppm	ppm	NOUN
eurjchem-1635	225	76	(	(	PUNCT
eurjchem-1635	225	77	strong	strong	ADJ
eurjchem-1635	225	78	)	)	PUNCT
eurjchem-1635	225	79	because	because	SCONJ
eurjchem-1635	225	80	proton	proton	NOUN
eurjchem-1635	225	81	at	at	ADP
eurjchem-1635	225	82	δ	δ	PROPN
eurjchem-1635	225	83	3.58	3.58	NUM
eurjchem-1635	225	84	ppm	ppm	NOUN
eurjchem-1635	225	85	is	be	AUX
eurjchem-1635	225	86	above	above	ADP
eurjchem-1635	225	87	the	the	DET
eurjchem-1635	225	88	plane	plane	NOUN
eurjchem-1635	225	89	and	and	CCONJ
eurjchem-1635	225	90	proton	proton	NOUN
eurjchem-1635	225	91	of	of	ADP
eurjchem-1635	225	92	δ	δ	PROPN
eurjchem-1635	225	93	3.42	3.42	NUM
eurjchem-1635	225	94	ppm	ppm	NOUN
eurjchem-1635	225	95	below	below	ADP
eurjchem-1635	225	96	the	the	DET
eurjchem-1635	225	97	plane	plane	NOUN
eurjchem-1635	225	98	.	.	PUNCT
eurjchem-1635	226	1	in	in	ADP
eurjchem-1635	226	2	second	second	ADJ
eurjchem-1635	226	3	noe	noe	PROPN
eurjchem-1635	226	4	experiment	experiment	NOUN
eurjchem-1635	226	5	,	,	PUNCT
eurjchem-1635	226	6	we	we	PRON
eurjchem-1635	226	7	have	have	AUX
eurjchem-1635	226	8	irradiated	irradiate	VERB
eurjchem-1635	226	9	proton	proton	NOUN
eurjchem-1635	226	10	at	at	ADP
eurjchem-1635	226	11	δ	δ	PROPN
eurjchem-1635	226	12	6.19	6.19	NUM
eurjchem-1635	226	13	ppm	ppm	NOUN
eurjchem-1635	226	14	(	(	PUNCT
eurjchem-1635	226	15	‐nh	‐nh	NOUN
eurjchem-1635	226	16	)	)	PUNCT
eurjchem-1635	226	17	,	,	PUNCT
eurjchem-1635	226	18	one	one	NUM
eurjchem-1635	226	19	aromatic	aromatic	ADJ
eurjchem-1635	226	20	proton	proton	NOUN
eurjchem-1635	226	21	at	at	ADP
eurjchem-1635	226	22	δ	δ	PROPN
eurjchem-1635	226	23	6.64	6.64	NUM
eurjchem-1635	226	24	ppm	ppm	NOUN
eurjchem-1635	226	25	next	next	ADV
eurjchem-1635	226	26	to	to	ADP
eurjchem-1635	226	27	‐nh	‐nh	NOUN
eurjchem-1635	226	28	shows	show	NOUN
eurjchem-1635	226	29	signal	signal	VERB
eurjchem-1635	226	30	along	along	ADP
eurjchem-1635	226	31	with	with	ADP
eurjchem-1635	226	32	δ	δ	PROPN
eurjchem-1635	226	33	3.58	3.58	NUM
eurjchem-1635	226	34	(	(	PUNCT
eurjchem-1635	226	35	strong	strong	ADJ
eurjchem-1635	226	36	)	)	PUNCT
eurjchem-1635	226	37	and	and	CCONJ
eurjchem-1635	226	38	3.42	3.42	NUM
eurjchem-1635	226	39	ppm	ppm	NOUN
eurjchem-1635	226	40	(	(	PUNCT
eurjchem-1635	226	41	weak	weak	ADJ
eurjchem-1635	226	42	)	)	PUNCT
eurjchem-1635	226	43	as	as	ADP
eurjchem-1635	226	44	‐nh	‐nh	NOUN
eurjchem-1635	226	45	and	and	CCONJ
eurjchem-1635	226	46	‐nh‐ch2	‐nh‐ch2	PROPN
eurjchem-1635	226	47	protons	proton	NOUN
eurjchem-1635	226	48	are	be	AUX
eurjchem-1635	226	49	in	in	ADP
eurjchem-1635	226	50	different	different	ADJ
eurjchem-1635	226	51	planes	plane	NOUN
eurjchem-1635	226	52	.	.	PUNCT
eurjchem-1635	227	1	in	in	ADP
eurjchem-1635	227	2	third	third	ADJ
eurjchem-1635	227	3	noe	noe	PROPN
eurjchem-1635	227	4	experiment	experiment	NOUN
eurjchem-1635	227	5	,	,	PUNCT
eurjchem-1635	227	6	we	we	PRON
eurjchem-1635	227	7	have	have	AUX
eurjchem-1635	227	8	irradiated	irradiate	VERB
eurjchem-1635	227	9	proton	proton	NOUN
eurjchem-1635	227	10	at	at	ADP
eurjchem-1635	227	11	δ	δ	PROPN
eurjchem-1635	227	12	3.58	3.58	NUM
eurjchem-1635	227	13	ppm	ppm	NOUN
eurjchem-1635	227	14	of	of	ADP
eurjchem-1635	227	15	(	(	PUNCT
eurjchem-1635	227	16	‐nh‐ch2	‐nh‐ch2	ADJ
eurjchem-1635	227	17	)	)	PUNCT
eurjchem-1635	227	18	protons	proton	NOUN
eurjchem-1635	227	19	at	at	ADP
eurjchem-1635	227	20	δ	δ	PROPN
eurjchem-1635	227	21	3.42	3.42	NUM
eurjchem-1635	227	22	ppm	ppm	NOUN
eurjchem-1635	227	23	shows	show	NOUN
eurjchem-1635	227	24	signal	signal	VERB
eurjchem-1635	227	25	along	along	ADP
eurjchem-1635	227	26	with	with	ADP
eurjchem-1635	227	27	δ	δ	PROPN
eurjchem-1635	227	28	6.19	6.19	NUM
eurjchem-1635	227	29	and	and	CCONJ
eurjchem-1635	227	30	5.57	5.57	NUM
eurjchem-1635	227	31	ppm	ppm	NOUN
eurjchem-1635	227	32	as	as	SCONJ
eurjchem-1635	227	33	both	both	PRON
eurjchem-1635	227	34	of	of	ADP
eurjchem-1635	227	35	these	these	PRON
eurjchem-1635	227	36	are	be	AUX
eurjchem-1635	227	37	adjacent	adjacent	ADJ
eurjchem-1635	227	38	to	to	ADP
eurjchem-1635	227	39	(	(	PUNCT
eurjchem-1635	227	40	‐nh‐ch2	‐nh‐ch2	ADJ
eurjchem-1635	227	41	)	)	PUNCT
eurjchem-1635	227	42	protons	proton	NOUN
eurjchem-1635	227	43	.	.	PUNCT
eurjchem-1635	228	1	from	from	ADP
eurjchem-1635	228	2	above	above	ADP
eurjchem-1635	228	3	three	three	NUM
eurjchem-1635	228	4	noe	noe	PROPN
eurjchem-1635	228	5	experiments	experiment	NOUN
eurjchem-1635	228	6	confirms	confirm	VERB
eurjchem-1635	228	7	,	,	PUNCT
eurjchem-1635	228	8	compound	compound	NOUN
eurjchem-1635	228	9	1	1	NUM
eurjchem-1635	228	10	as	as	ADP
eurjchem-1635	228	11	desired	desire	VERB
eurjchem-1635	228	12	product	product	NOUN
eurjchem-1635	228	13	.	.	PUNCT
eurjchem-1635	229	1	in	in	ADP
eurjchem-1635	229	2	all	all	DET
eurjchem-1635	229	3	optimization	optimization	NOUN
eurjchem-1635	229	4	reactions	reaction	NOUN
eurjchem-1635	229	5	major	major	ADJ
eurjchem-1635	229	6	side	side	NOUN
eurjchem-1635	229	7	product	product	NOUN
eurjchem-1635	229	8	is	be	AUX
eurjchem-1635	229	9	compound	compound	NOUN
eurjchem-1635	229	10	1a	1a	NOUN
eurjchem-1635	229	11	,	,	PUNCT
eurjchem-1635	229	12	with	with	ADP
eurjchem-1635	229	13	the	the	DET
eurjchem-1635	229	14	yields	yield	NOUN
eurjchem-1635	229	15	of	of	ADP
eurjchem-1635	229	16	10	10	NUM
eurjchem-1635	229	17	to	to	PART
eurjchem-1635	229	18	51	51	NUM
eurjchem-1635	229	19	%	%	NOUN
eurjchem-1635	229	20	.	.	PUNCT
eurjchem-1635	230	1	in	in	ADP
eurjchem-1635	230	2	entry	entry	NOUN
eurjchem-1635	230	3	6	6	NUM
eurjchem-1635	230	4	,	,	PUNCT
eurjchem-1635	230	5	when	when	SCONJ
eurjchem-1635	230	6	we	we	PRON
eurjchem-1635	230	7	use	use	VERB
eurjchem-1635	230	8	cs2co3	cs2co3	VERB
eurjchem-1635	230	9	with	with	ADP
eurjchem-1635	230	10	toluene	toluene	NOUN
eurjchem-1635	230	11	at	at	ADP
eurjchem-1635	230	12	110	110	NUM
eurjchem-1635	230	13	°	°	NOUN
eurjchem-1635	230	14	c	c	NOUN
eurjchem-1635	230	15	for	for	ADP
eurjchem-1635	230	16	12	12	NUM
eurjchem-1635	230	17	h	h	NOUN
eurjchem-1635	230	18	,	,	PUNCT
eurjchem-1635	230	19	there	there	PRON
eurjchem-1635	230	20	is	be	VERB
eurjchem-1635	230	21	70	70	NUM
eurjchem-1635	230	22	%	%	NOUN
eurjchem-1635	230	23	formation	formation	NOUN
eurjchem-1635	230	24	of	of	ADP
eurjchem-1635	230	25	product	product	NOUN
eurjchem-1635	230	26	1	1	NUM
eurjchem-1635	230	27	and	and	CCONJ
eurjchem-1635	230	28	10	10	NUM
eurjchem-1635	230	29	%	%	NOUN
eurjchem-1635	230	30	formation	formation	NOUN
eurjchem-1635	230	31	of	of	ADP
eurjchem-1635	230	32	compound	compound	NOUN
eurjchem-1635	230	33	1a	1a	NOUN
eurjchem-1635	230	34	.	.	PUNCT
eurjchem-1635	231	1	further	far	ADV
eurjchem-1635	231	2	,	,	PUNCT
eurjchem-1635	231	3	we	we	PRON
eurjchem-1635	231	4	have	have	AUX
eurjchem-1635	231	5	explored	explore	VERB
eurjchem-1635	231	6	this	this	DET
eurjchem-1635	231	7	condition	condition	NOUN
eurjchem-1635	231	8	to	to	PART
eurjchem-1635	231	9	increase	increase	VERB
eurjchem-1635	231	10	the	the	DET
eurjchem-1635	231	11	yield	yield	NOUN
eurjchem-1635	231	12	of	of	ADP
eurjchem-1635	231	13	compound	compound	NOUN
eurjchem-1635	231	14	1	1	NUM
eurjchem-1635	231	15	.	.	PUNCT
eurjchem-1635	232	1	we	we	PRON
eurjchem-1635	232	2	have	have	AUX
eurjchem-1635	232	3	modified	modify	VERB
eurjchem-1635	232	4	condition	condition	NOUN
eurjchem-1635	232	5	by	by	ADP
eurjchem-1635	232	6	pre‐	pre‐	NOUN
eurjchem-1635	232	7	paring	paring	NOUN
eurjchem-1635	232	8	anion	anion	NOUN
eurjchem-1635	232	9	by	by	ADP
eurjchem-1635	232	10	heating	heat	VERB
eurjchem-1635	232	11	2‐amino	2‐amino	NUM
eurjchem-1635	232	12	phenol	phenol	NOUN
eurjchem-1635	232	13	with	with	ADP
eurjchem-1635	232	14	cs2co3	cs2co3	VERB
eurjchem-1635	232	15	at	at	ADP
eurjchem-1635	232	16	60	60	NUM
eurjchem-1635	232	17	°	°	ADP
eurjchem-1635	232	18	c	c	NOUN
eurjchem-1635	232	19	for	for	ADP
eurjchem-1635	232	20	0.5	0.5	NUM
eurjchem-1635	232	21	h	h	NOUN
eurjchem-1635	232	22	then	then	ADV
eurjchem-1635	232	23	adding	add	VERB
eurjchem-1635	232	24	the	the	DET
eurjchem-1635	232	25	2‐chloroacrylonitrile	2‐chloroacrylonitrile	ADJ
eurjchem-1635	232	26	and	and	CCONJ
eurjchem-1635	232	27	further	far	ADV
eurjchem-1635	232	28	heating	heating	NOUN
eurjchem-1635	232	29	at	at	ADP
eurjchem-1635	232	30	110	110	NUM
eurjchem-1635	232	31	°	°	NOUN
eurjchem-1635	232	32	c	c	NOUN
eurjchem-1635	232	33	for	for	ADP
eurjchem-1635	232	34	4	4	NUM
eurjchem-1635	232	35	h	h	NOUN
eurjchem-1635	232	36	there	there	PRON
eurjchem-1635	232	37	is	be	VERB
eurjchem-1635	232	38	90	90	NUM
eurjchem-1635	232	39	%	%	NOUN
eurjchem-1635	232	40	formation	formation	NOUN
eurjchem-1635	232	41	of	of	ADP
eurjchem-1635	232	42	compound	compound	NOUN
eurjchem-1635	232	43	1	1	NUM
eurjchem-1635	232	44	and	and	CCONJ
eurjchem-1635	232	45	3	3	NUM
eurjchem-1635	232	46	%	%	NOUN
eurjchem-1635	232	47	formation	formation	NOUN
eurjchem-1635	232	48	of	of	ADP
eurjchem-1635	232	49	compound	compound	NOUN
eurjchem-1635	232	50	1a	1a	NOUN
eurjchem-1635	232	51	.	.	PUNCT
eurjchem-1635	233	1	for	for	ADP
eurjchem-1635	233	2	step	step	NOUN
eurjchem-1635	233	3	(	(	PUNCT
eurjchem-1635	233	4	a	a	NOUN
eurjchem-1635	233	5	)	)	PUNCT
eurjchem-1635	233	6	in	in	ADP
eurjchem-1635	233	7	scheme	scheme	NOUN
eurjchem-1635	233	8	2	2	NUM
eurjchem-1635	233	9	,	,	PUNCT
eurjchem-1635	233	10	we	we	PRON
eurjchem-1635	233	11	treated	treat	VERB
eurjchem-1635	233	12	2‐amino	2‐amino	NUM
eurjchem-1635	233	13	phenol	phenol	NOUN
eurjchem-1635	233	14	with	with	ADP
eurjchem-1635	233	15	cs2co3	cs2co3	VERB
eurjchem-1635	233	16	at	at	ADP
eurjchem-1635	233	17	60	60	NUM
eurjchem-1635	233	18	°	°	ADP
eurjchem-1635	233	19	c	c	NOUN
eurjchem-1635	233	20	for	for	ADP
eurjchem-1635	233	21	0.5	0.5	NUM
eurjchem-1635	233	22	h	h	NOUN
eurjchem-1635	233	23	then	then	ADV
eurjchem-1635	233	24	adding	add	VERB
eurjchem-1635	233	25	the	the	DET
eurjchem-1635	233	26	2‐chloromethylacrylonitrile	2‐chloromethylacrylonitrile	NOUN
eurjchem-1635	233	27	and	and	CCONJ
eurjchem-1635	233	28	further	far	ADV
eurjchem-1635	233	29	heating	heating	NOUN
eurjchem-1635	233	30	at	at	ADP
eurjchem-1635	233	31	110	110	NUM
eurjchem-1635	233	32	°	°	NOUN
eurjchem-1635	233	33	c	c	NOUN
eurjchem-1635	233	34	for	for	ADP
eurjchem-1635	233	35	4	4	NUM
eurjchem-1635	233	36	h	h	NOUN
eurjchem-1635	233	37	,	,	PUNCT
eurjchem-1635	233	38	there	there	PRON
eurjchem-1635	233	39	is	be	VERB
eurjchem-1635	233	40	87	87	NUM
eurjchem-1635	233	41	%	%	NOUN
eurjchem-1635	233	42	formation	formation	NOUN
eurjchem-1635	233	43	of	of	ADP
eurjchem-1635	233	44	compound	compound	NOUN
eurjchem-1635	233	45	5	5	NUM
eurjchem-1635	233	46	and	and	CCONJ
eurjchem-1635	233	47	5	5	NUM
eurjchem-1635	233	48	%	%	NOUN
eurjchem-1635	233	49	formation	formation	NOUN
eurjchem-1635	233	50	of	of	ADP
eurjchem-1635	233	51	compound	compound	NOUN
eurjchem-1635	233	52	1a	1a	NOUN
eurjchem-1635	233	53	.	.	PUNCT
eurjchem-1635	234	1	for	for	ADP
eurjchem-1635	234	2	step	step	NOUN
eurjchem-1635	234	3	(	(	PUNCT
eurjchem-1635	234	4	b	b	NOUN
eurjchem-1635	234	5	)	)	PUNCT
eurjchem-1635	234	6	,	,	PUNCT
eurjchem-1635	234	7	again	again	ADV
eurjchem-1635	234	8	,	,	PUNCT
eurjchem-1635	234	9	we	we	PRON
eurjchem-1635	234	10	have	have	AUX
eurjchem-1635	234	11	optimized	optimize	VERB
eurjchem-1635	234	12	the	the	DET
eurjchem-1635	234	13	condition	condition	NOUN
eurjchem-1635	234	14	as	as	SCONJ
eurjchem-1635	234	15	mentioned	mention	VERB
eurjchem-1635	234	16	in	in	ADP
eurjchem-1635	234	17	table	table	NOUN
eurjchem-1635	234	18	2	2	NUM
eurjchem-1635	234	19	by	by	ADP
eurjchem-1635	234	20	taking	take	VERB
eurjchem-1635	234	21	compound	compound	NOUN
eurjchem-1635	234	22	1	1	NUM
eurjchem-1635	234	23	and	and	CCONJ
eurjchem-1635	234	24	5	5	NUM
eurjchem-1635	234	25	(	(	PUNCT
eurjchem-1635	234	26	1	1	NUM
eurjchem-1635	234	27	equiv	equiv	NOUN
eurjchem-1635	234	28	.	.	PUNCT
eurjchem-1635	234	29	)	)	PUNCT
eurjchem-1635	235	1	and	and	CCONJ
eurjchem-1635	235	2	reacting	react	VERB
eurjchem-1635	235	3	it	it	PRON
eurjchem-1635	235	4	with	with	ADP
eurjchem-1635	235	5	benzyl	benzyl	NOUN
eurjchem-1635	235	6	bromide	bromide	NOUN
eurjchem-1635	235	7	and	and	CCONJ
eurjchem-1635	235	8	phenylmethanethiol	phenylmethanethiol	PROPN
eurjchem-1635	235	9	(	(	PUNCT
eurjchem-1635	235	10	1.2	1.2	NUM
eurjchem-1635	235	11	equiv	equiv	NOUN
eurjchem-1635	235	12	.	.	PUNCT
eurjchem-1635	235	13	)	)	PUNCT
eurjchem-1635	236	1	each	each	PRON
eurjchem-1635	236	2	.	.	PUNCT
eurjchem-1635	237	1	we	we	PRON
eurjchem-1635	237	2	have	have	VERB
eurjchem-1635	237	3	optimized	optimize	VERB
eurjchem-1635	237	4	base	base	NOUN
eurjchem-1635	237	5	,	,	PUNCT
eurjchem-1635	237	6	solvents	solvent	NOUN
eurjchem-1635	237	7	,	,	PUNCT
eurjchem-1635	237	8	temperature	temperature	NOUN
eurjchem-1635	237	9	and	and	CCONJ
eurjchem-1635	237	10	time	time	NOUN
eurjchem-1635	237	11	for	for	ADP
eurjchem-1635	237	12	getting	get	VERB
eurjchem-1635	237	13	better	well	ADJ
eurjchem-1635	237	14	yields	yield	NOUN
eurjchem-1635	237	15	for	for	ADP
eurjchem-1635	237	16	step	step	NOUN
eurjchem-1635	237	17	(	(	PUNCT
eurjchem-1635	237	18	b	b	NOUN
eurjchem-1635	237	19	)	)	PUNCT
eurjchem-1635	237	20	.	.	PUNCT
eurjchem-1635	238	1	all	all	DET
eurjchem-1635	238	2	reactions	reaction	NOUN
eurjchem-1635	238	3	were	be	AUX
eurjchem-1635	238	4	initially	initially	ADV
eurjchem-1635	238	5	done	do	VERB
eurjchem-1635	238	6	from	from	ADP
eurjchem-1635	238	7	0	0	NUM
eurjchem-1635	238	8	°	°	ADP
eurjchem-1635	238	9	c	c	NOUN
eurjchem-1635	238	10	to	to	PART
eurjchem-1635	238	11	room	room	VERB
eurjchem-1635	238	12	temperature	temperature	NOUN
eurjchem-1635	238	13	for	for	ADP
eurjchem-1635	238	14	6	6	NUM
eurjchem-1635	238	15	h	h	NOUN
eurjchem-1635	238	16	(	(	PUNCT
eurjchem-1635	238	17	table	table	NOUN
eurjchem-1635	238	18	2	2	NUM
eurjchem-1635	238	19	,	,	PUNCT
eurjchem-1635	238	20	entries	entry	NOUN
eurjchem-1635	238	21	1	1	NUM
eurjchem-1635	238	22	to	to	PART
eurjchem-1635	238	23	5	5	NUM
eurjchem-1635	238	24	)	)	PUNCT
eurjchem-1635	238	25	on	on	ADP
eurjchem-1635	238	26	tlc	tlc	PROPN
eurjchem-1635	238	27	,	,	PUNCT
eurjchem-1635	238	28	there	there	PRON
eurjchem-1635	238	29	is	be	VERB
eurjchem-1635	238	30	majority	majority	NOUN
eurjchem-1635	238	31	of	of	ADP
eurjchem-1635	238	32	starting	start	VERB
eurjchem-1635	238	33	remains	remain	NOUN
eurjchem-1635	238	34	as	as	ADP
eurjchem-1635	238	35	such	such	ADJ
eurjchem-1635	238	36	then	then	ADV
eurjchem-1635	238	37	we	we	PRON
eurjchem-1635	238	38	applied	apply	VERB
eurjchem-1635	238	39	heating	heat	VERB
eurjchem-1635	238	40	them	they	PRON
eurjchem-1635	238	41	for	for	ADP
eurjchem-1635	238	42	remaining	remain	VERB
eurjchem-1635	238	43	time	time	NOUN
eurjchem-1635	238	44	at	at	ADP
eurjchem-1635	238	45	70	70	NUM
eurjchem-1635	238	46	°	°	NOUN
eurjchem-1635	238	47	c	c	NOUN
eurjchem-1635	238	48	the	the	DET
eurjchem-1635	238	49	yields	yield	NOUN
eurjchem-1635	238	50	are	be	AUX
eurjchem-1635	238	51	in	in	ADP
eurjchem-1635	238	52	between	between	ADP
eurjchem-1635	238	53	20‐60	20‐60	NUM
eurjchem-1635	238	54	%	%	NOUN
eurjchem-1635	238	55	.	.	PUNCT
eurjchem-1635	239	1	but	but	CCONJ
eurjchem-1635	239	2	,	,	PUNCT
eurjchem-1635	239	3	in	in	ADP
eurjchem-1635	239	4	entries	entry	NOUN
eurjchem-1635	239	5	6	6	NUM
eurjchem-1635	239	6	and	and	CCONJ
eurjchem-1635	239	7	7	7	NUM
eurjchem-1635	239	8	,	,	PUNCT
eurjchem-1635	239	9	we	we	PRON
eurjchem-1635	239	10	directly	directly	ADV
eurjchem-1635	239	11	heated	heat	VERB
eurjchem-1635	239	12	reaction	reaction	NOUN
eurjchem-1635	239	13	mixture	mixture	NOUN
eurjchem-1635	239	14	for	for	ADP
eurjchem-1635	239	15	4	4	NUM
eurjchem-1635	239	16	h	h	NOUN
eurjchem-1635	239	17	the	the	DET
eurjchem-1635	239	18	yield	yield	NOUN
eurjchem-1635	239	19	obtained	obtain	VERB
eurjchem-1635	239	20	of	of	ADP
eurjchem-1635	239	21	the	the	DET
eurjchem-1635	239	22	product	product	NOUN
eurjchem-1635	239	23	was	be	AUX
eurjchem-1635	239	24	60	60	NUM
eurjchem-1635	239	25	and	and	CCONJ
eurjchem-1635	239	26	55	55	NUM
eurjchem-1635	239	27	%	%	NOUN
eurjchem-1635	239	28	,	,	PUNCT
eurjchem-1635	239	29	respectively	respectively	ADV
eurjchem-1635	239	30	.	.	PUNCT
eurjchem-1635	240	1	pawar	pawar	PROPN
eurjchem-1635	240	2	et	et	PROPN
eurjchem-1635	240	3	al	al	PROPN
eurjchem-1635	240	4	.	.	PUNCT
eurjchem-1635	240	5	/	/	SYM
eurjchem-1635	240	6	european	european	PROPN
eurjchem-1635	240	7	journal	journal	PROPN
eurjchem-1635	240	8	of	of	ADP
eurjchem-1635	240	9	chemistry	chemistry	NOUN
eurjchem-1635	240	10	8	8	NUM
eurjchem-1635	240	11	(	(	PUNCT
eurjchem-1635	240	12	4	4	NUM
eurjchem-1635	240	13	)	)	PUNCT
eurjchem-1635	240	14	(	(	PUNCT
eurjchem-1635	240	15	2017	2017	NUM
eurjchem-1635	240	16	)	)	PUNCT
eurjchem-1635	240	17	384‐390	384‐390	NUM
eurjchem-1635	240	18	389	389	NUM
eurjchem-1635	240	19	table	table	NOUN
eurjchem-1635	240	20	2	2	NUM
eurjchem-1635	240	21	.	.	PUNCT
eurjchem-1635	240	22	screening	screen	VERB
eurjchem-1635	240	23	conditions	condition	NOUN
eurjchem-1635	240	24	for	for	ADP
eurjchem-1635	240	25	step	step	NOUN
eurjchem-1635	240	26	(	(	PUNCT
eurjchem-1635	240	27	b	b	NOUN
eurjchem-1635	240	28	)	)	PUNCT
eurjchem-1635	240	29	in	in	ADP
eurjchem-1635	240	30	scheme	scheme	NOUN
eurjchem-1635	240	31	1	1	NUM
eurjchem-1635	240	32	.	.	PUNCT
eurjchem-1635	240	33	entry	entry	NOUN
eurjchem-1635	240	34	base	base	NOUN
eurjchem-1635	240	35	solvent	solvent	NOUN
eurjchem-1635	240	36	temperature	temperature	NOUN
eurjchem-1635	240	37	(	(	PUNCT
eurjchem-1635	240	38	°	°	ADP
eurjchem-1635	240	39	c	c	NOUN
eurjchem-1635	240	40	)	)	PUNCT
eurjchem-1635	240	41	time	time	NOUN
eurjchem-1635	240	42	(	(	PUNCT
eurjchem-1635	240	43	h	h	NOUN
eurjchem-1635	240	44	)	)	PUNCT
eurjchem-1635	240	45	yield	yield	NOUN
eurjchem-1635	240	46	(	(	PUNCT
eurjchem-1635	240	47	%	%	INTJ
eurjchem-1635	240	48	)	)	PUNCT
eurjchem-1635	240	49	a	a	PRON
eurjchem-1635	240	50	,	,	PUNCT
eurjchem-1635	240	51	compound	compound	NOUN
eurjchem-1635	240	52	2	2	NUM
eurjchem-1635	240	53	and	and	CCONJ
eurjchem-1635	240	54	6	6	NUM
eurjchem-1635	240	55	1	1	NUM
eurjchem-1635	240	56	tea	tea	NOUN
eurjchem-1635	240	57	thf	thf	NOUN
eurjchem-1635	240	58	0	0	PUNCT
eurjchem-1635	240	59	to	to	ADP
eurjchem-1635	240	60	70	70	NUM
eurjchem-1635	240	61	12	12	NUM
eurjchem-1635	240	62	30	30	NUM
eurjchem-1635	240	63	,	,	PUNCT
eurjchem-1635	240	64	15	15	NUM
eurjchem-1635	240	65	2	2	NUM
eurjchem-1635	240	66	pyridine	pyridine	NOUN
eurjchem-1635	240	67	thf	thf	NOUN
eurjchem-1635	240	68	0	0	NUM
eurjchem-1635	240	69	to	to	ADP
eurjchem-1635	240	70	70	70	NUM
eurjchem-1635	240	71	8	8	NUM
eurjchem-1635	240	72	25	25	NUM
eurjchem-1635	240	73	,	,	PUNCT
eurjchem-1635	240	74	na	na	NOUN
eurjchem-1635	240	75	3	3	NUM
eurjchem-1635	240	76	dipea	dipea	NOUN
eurjchem-1635	240	77	thf	thf	NOUN
eurjchem-1635	240	78	0	0	NUM
eurjchem-1635	240	79	to	to	ADP
eurjchem-1635	240	80	70	70	NUM
eurjchem-1635	240	81	12	12	NUM
eurjchem-1635	240	82	20	20	NUM
eurjchem-1635	240	83	,	,	PUNCT
eurjchem-1635	240	84	na	na	ADP
eurjchem-1635	240	85	4	4	NUM
eurjchem-1635	240	86	2,6‐lutidine	2,6‐lutidine	NUM
eurjchem-1635	240	87	thf	thf	NOUN
eurjchem-1635	240	88	0	0	PUNCT
eurjchem-1635	240	89	to	to	ADP
eurjchem-1635	240	90	70	70	NUM
eurjchem-1635	240	91	12	12	NUM
eurjchem-1635	240	92	25	25	NUM
eurjchem-1635	240	93	,	,	PUNCT
eurjchem-1635	240	94	8	8	NUM
eurjchem-1635	240	95	5	5	NUM
eurjchem-1635	240	96	2,6‐lutidine	2,6‐lutidine	NUM
eurjchem-1635	240	97	dmf	dmf	X
eurjchem-1635	240	98	0	0	NUM
eurjchem-1635	240	99	to	to	ADP
eurjchem-1635	240	100	70	70	NUM
eurjchem-1635	240	101	12	12	NUM
eurjchem-1635	240	102	40	40	NUM
eurjchem-1635	240	103	,	,	PUNCT
eurjchem-1635	240	104	15	15	NUM
eurjchem-1635	240	105	6	6	NUM
eurjchem-1635	240	106	2,6‐lutidine+dmap	2,6‐lutidine+dmap	NUM
eurjchem-1635	240	107	acetone	acetone	NOUN
eurjchem-1635	240	108	0	0	NUM
eurjchem-1635	240	109	to	to	ADP
eurjchem-1635	240	110	70	70	NUM
eurjchem-1635	240	111	4	4	NUM
eurjchem-1635	240	112	60	60	NUM
eurjchem-1635	240	113	,	,	PUNCT
eurjchem-1635	240	114	20	20	NUM
eurjchem-1635	240	115	7	7	NUM
eurjchem-1635	240	116	2,6‐lutidine+dmap	2,6‐lutidine+dmap	NUM
eurjchem-1635	240	117	acetone	acetone	NOUN
eurjchem-1635	240	118	0	0	NUM
eurjchem-1635	240	119	to	to	ADP
eurjchem-1635	240	120	70	70	NUM
eurjchem-1635	240	121	4	4	NUM
eurjchem-1635	240	122	55	55	NUM
eurjchem-1635	240	123	,	,	PUNCT
eurjchem-1635	240	124	16	16	NUM
eurjchem-1635	240	125	8	8	NUM
eurjchem-1635	240	126	2,6‐lutidine+dmap	2,6‐lutidine+dmap	NUM
eurjchem-1635	240	127	acetone	acetone	NOUN
eurjchem-1635	240	128	0	0	NUM
eurjchem-1635	240	129	to	to	ADP
eurjchem-1635	240	130	80	80	NUM
eurjchem-1635	240	131	1	1	NUM
eurjchem-1635	240	132	85	85	NUM
eurjchem-1635	240	133	,	,	PUNCT
eurjchem-1635	240	134	21	21	NUM
eurjchem-1635	240	135	a	a	DET
eurjchem-1635	240	136	isolated	isolated	ADJ
eurjchem-1635	240	137	yield	yield	NOUN
eurjchem-1635	240	138	.	.	PUNCT
eurjchem-1635	241	1	table	table	NOUN
eurjchem-1635	241	2	3	3	NUM
eurjchem-1635	241	3	.	.	PUNCT
eurjchem-1635	242	1	in	in	ADP
eurjchem-1635	242	2	vitro	vitro	X
eurjchem-1635	242	3	anticancer	anticancer	NOUN
eurjchem-1635	242	4	screening	screening	NOUN
eurjchem-1635	242	5	of	of	ADP
eurjchem-1635	242	6	the	the	DET
eurjchem-1635	242	7	synthesized	synthesize	VERB
eurjchem-1635	242	8	compounds	compound	NOUN
eurjchem-1635	242	9	against	against	ADP
eurjchem-1635	242	10	five	five	NUM
eurjchem-1635	242	11	cell	cell	NOUN
eurjchem-1635	242	12	lines	line	NOUN
eurjchem-1635	242	13	.	.	PUNCT
eurjchem-1635	243	1	compound	compound	VERB
eurjchem-1635	243	2	a‐549	a‐549	PRON
eurjchem-1635	243	3	a	a	DET
eurjchem-1635	243	4	sif	sif	PROPN
eurjchem-1635	243	5	hela	hela	PROPN
eurjchem-1635	243	6	b	b	PROPN
eurjchem-1635	243	7	si	si	PROPN
eurjchem-1635	243	8	f	f	X
eurjchem-1635	243	9	mcf‐7	mcf‐7	PROPN
eurjchem-1635	243	10	c	c	PROPN
eurjchem-1635	243	11	si	si	PROPN
eurjchem-1635	243	12	f	f	PROPN
eurjchem-1635	243	13	du‐145	du‐145	PROPN
eurjchem-1635	244	1	d	d	PROPN
eurjchem-1635	244	2	si	si	PROPN
eurjchem-1635	244	3	f	f	PROPN
eurjchem-1635	244	4	huvec	huvec	PROPN
eurjchem-1635	244	5	e	e	PROPN
eurjchem-1635	244	6	4a	4a	NOUN
eurjchem-1635	244	7	22.72±0.11	22.72±0.11	PROPN
eurjchem-1635	244	8	4.03	4.03	NUM
eurjchem-1635	244	9	23.87±0.08	23.87±0.08	NUM
eurjchem-1635	244	10	3.83	3.83	NUM
eurjchem-1635	244	11	24.12±0.06	24.12±0.06	NUM
eurjchem-1635	244	12	3.79	3.79	NUM
eurjchem-1635	244	13	28.86±0.22	28.86±0.22	NUM
eurjchem-1635	244	14	3.17	3.17	NUM
eurjchem-1635	244	15	91.6±0.28	91.6±0.28	NUM
eurjchem-1635	244	16	4b	4b	NOUN
eurjchem-1635	244	17	33.81±0.11	33.81±0.11	NUM
eurjchem-1635	244	18	2.94	2.94	NUM
eurjchem-1635	244	19	24.32±0.04	24.32±0.04	NUM
eurjchem-1635	244	20	4.09	4.09	NUM
eurjchem-1635	244	21	25.32±0.06	25.32±0.06	NUM
eurjchem-1635	244	22	3.93	3.93	NUM
eurjchem-1635	244	23	23.73±0.12	23.73±0.12	NUM
eurjchem-1635	244	24	4.19	4.19	NUM
eurjchem-1635	244	25	99.6±0.14	99.6±0.14	NUM
eurjchem-1635	244	26	4c	4c	NOUN
eurjchem-1635	244	27	10.81±0.11	10.81±0.11	NUM
eurjchem-1635	244	28	8.85	8.85	NUM
eurjchem-1635	244	29	28.32±0.04	28.32±0.04	NUM
eurjchem-1635	244	30	3.37	3.37	NUM
eurjchem-1635	244	31	27.32±0.06	27.32±0.06	NUM
eurjchem-1635	244	32	3.50	3.50	NUM
eurjchem-1635	244	33	20.73±0.12	20.73±0.12	NUM
eurjchem-1635	244	34	4.61	4.61	NUM
eurjchem-1635	244	35	95.7±0.28	95.7±0.28	NUM
eurjchem-1635	244	36	4d	4d	NOUN
eurjchem-1635	244	37	10.65±0.11	10.65±0.11	NUM
eurjchem-1635	244	38	8.78	8.78	NUM
eurjchem-1635	244	39	10.79±0.22	10.79±0.22	NUM
eurjchem-1635	244	40	8.67	8.67	NUM
eurjchem-1635	244	41	12.86±0.12	12.86±0.12	NUM
eurjchem-1635	244	42	7.27	7.27	NUM
eurjchem-1635	244	43	10.82±0.11	10.82±0.11	NUM
eurjchem-1635	244	44	8.65	8.65	NUM
eurjchem-1635	244	45	93.6±0.28	93.6±0.28	NUM
eurjchem-1635	244	46	4e	4e	NOUN
eurjchem-1635	244	47	23.86±0.08	23.86±0.08	NUM
eurjchem-1635	244	48	3.96	3.96	NUM
eurjchem-1635	244	49	14.38±0.06	14.38±0.06	NUM
eurjchem-1635	244	50	6.57	6.57	NUM
eurjchem-1635	244	51	23.63±0.12	23.63±0.12	NUM
eurjchem-1635	244	52	4.00	4.00	NUM
eurjchem-1635	244	53	21.52±0.22	21.52±0.22	NUM
eurjchem-1635	244	54	4.39	4.39	NUM
eurjchem-1635	244	55	94.6±0.12	94.6±0.12	NUM
eurjchem-1635	244	56	7a	7a	NOUN
eurjchem-1635	244	57	25.72±0.11	25.72±0.11	NUM
eurjchem-1635	244	58	3.71	3.71	NUM
eurjchem-1635	244	59	26.87±0.08	26.87±0.08	NUM
eurjchem-1635	244	60	3.55	3.55	NUM
eurjchem-1635	244	61	24.12±0.06	24.12±0.06	NUM
eurjchem-1635	244	62	3.96	3.96	NUM
eurjchem-1635	244	63	28.86±0.22	28.86±0.22	NUM
eurjchem-1635	244	64	3.31	3.31	NUM
eurjchem-1635	244	65	95.6±0.28	95.6±0.28	NUM
eurjchem-1635	244	66	7b	7b	NOUN
eurjchem-1635	244	67	33.82±0.11	33.82±0.11	NUM
eurjchem-1635	244	68	2.61	2.61	NUM
eurjchem-1635	244	69	21.99±0.22	21.99±0.22	NUM
eurjchem-1635	244	70	4.00	4.00	NUM
eurjchem-1635	244	71	20.36±0.12	20.36±0.12	NUM
eurjchem-1635	244	72	4.35	4.35	NUM
eurjchem-1635	244	73	22.52±0.11	22.52±0.11	NUM
eurjchem-1635	244	74	3.93	3.93	NUM
eurjchem-1635	244	75	88.6±0.28	88.6±0.28	NUM
eurjchem-1635	244	76	7c	7c	X
eurjchem-1635	244	77	10.78±0.14	10.78±0.14	NUM
eurjchem-1635	244	78	9.23	9.23	NUM
eurjchem-1635	244	79	10.78±0.08	10.78±0.08	NUM
eurjchem-1635	244	80	9.23	9.23	NUM
eurjchem-1635	244	81	13.82±0.08	13.82±0.08	NUM
eurjchem-1635	244	82	7.20	7.20	NUM
eurjchem-1635	244	83	14.72±0.06	14.72±0.06	NUM
eurjchem-1635	244	84	6.76	6.76	NUM
eurjchem-1635	244	85	96.6±0.19	96.6±0.19	NUM
eurjchem-1635	244	86	7d	7d	NUM
eurjchem-1635	244	87	10.82±0.11	10.82±0.11	NUM
eurjchem-1635	244	88	9.15	9.15	NUM
eurjchem-1635	244	89	10.99±0.22	10.99±0.22	NUM
eurjchem-1635	244	90	9.01	9.01	NUM
eurjchem-1635	244	91	12.36±0.12	12.36±0.12	NUM
eurjchem-1635	244	92	8.01	8.01	NUM
eurjchem-1635	244	93	19.52±0.11	19.52±0.11	NUM
eurjchem-1635	244	94	5.07	5.07	NUM
eurjchem-1635	244	95	99.1±0.26	99.1±0.26	NUM
eurjchem-1635	244	96	7e	7e	NOUN
eurjchem-1635	244	97	24.13±0.12	24.13±0.12	NUM
eurjchem-1635	244	98	3.71	3.71	NUM
eurjchem-1635	244	99	25.16±0.08	25.16±0.08	NUM
eurjchem-1635	244	100	3.56	3.56	NUM
eurjchem-1635	244	101	26.12±0.12	26.12±0.12	NUM
eurjchem-1635	244	102	3.43	3.43	NUM
eurjchem-1635	244	103	21.62±0.11	21.62±0.11	NUM
eurjchem-1635	244	104	4.14	4.14	NUM
eurjchem-1635	244	105	89.6±0.22	89.6±0.22	NUM
eurjchem-1635	244	106	5‐fu	5‐fu	NUM
eurjchem-1635	244	107	1.71±0.11	1.71±0.11	NUM
eurjchem-1635	244	108	46.54	46.54	NUM
eurjchem-1635	244	109	1.82±0.13	1.82±0.13	NUM
eurjchem-1635	244	110	43.73	43.73	NUM
eurjchem-1635	244	111	1.91±0.08	1.91±0.08	NUM
eurjchem-1635	244	112	41.67	41.67	NUM
eurjchem-1635	244	113	1.82±0.08	1.82±0.08	NUM
eurjchem-1635	244	114	43.73	43.73	NUM
eurjchem-1635	244	115	79.6±0.18	79.6±0.18	NUM
eurjchem-1635	244	116	a	a	DET
eurjchem-1635	244	117	a‐549	a‐549	NOUN
eurjchem-1635	244	118	:	:	PUNCT
eurjchem-1635	244	119	human	human	ADJ
eurjchem-1635	244	120	lung	lung	NOUN
eurjchem-1635	244	121	cancer	cancer	NOUN
eurjchem-1635	244	122	cell	cell	NOUN
eurjchem-1635	244	123	line	line	NOUN
eurjchem-1635	244	124	.	.	PUNCT
eurjchem-1635	245	1	b	b	X
eurjchem-1635	245	2	hela	hela	ADJ
eurjchem-1635	245	3	:	:	PUNCT
eurjchem-1635	245	4	human	human	ADJ
eurjchem-1635	245	5	cervical	cervical	ADJ
eurjchem-1635	245	6	cancer	cancer	NOUN
eurjchem-1635	245	7	cell	cell	NOUN
eurjchem-1635	245	8	line	line	NOUN
eurjchem-1635	245	9	(	(	PUNCT
eurjchem-1635	245	10	atcc	atcc	ADJ
eurjchem-1635	245	11	ccl‐2	ccl‐2	PROPN
eurjchem-1635	245	12	)	)	PUNCT
eurjchem-1635	245	13	.	.	PUNCT
eurjchem-1635	246	1	c	c	PROPN
eurjchem-1635	247	1	mcf‐7	mcf‐7	NOUN
eurjchem-1635	247	2	:	:	PUNCT
eurjchem-1635	247	3	human	human	ADJ
eurjchem-1635	247	4	breast	breast	NOUN
eurjchem-1635	247	5	cancer	cancer	NOUN
eurjchem-1635	247	6	cell	cell	NOUN
eurjchem-1635	247	7	line	line	NOUN
eurjchem-1635	247	8	.	.	PUNCT
eurjchem-1635	248	1	d	d	X
eurjchem-1635	248	2	du‐145	du‐145	NOUN
eurjchem-1635	248	3	:	:	PUNCT
eurjchem-1635	248	4	human	human	ADJ
eurjchem-1635	248	5	prostate	prostate	NOUN
eurjchem-1635	248	6	cancer	cancer	NOUN
eurjchem-1635	248	7	cell	cell	NOUN
eurjchem-1635	248	8	line	line	NOUN
eurjchem-1635	248	9	.	.	PUNCT
eurjchem-1635	249	1	e	e	NOUN
eurjchem-1635	249	2	huvec	huvec	NOUN
eurjchem-1635	249	3	:	:	PUNCT
eurjchem-1635	249	4	human	human	ADJ
eurjchem-1635	249	5	umbilical	umbilical	ADJ
eurjchem-1635	249	6	vein	vein	ADJ
eurjchem-1635	249	7	endothelial	endothelial	ADJ
eurjchem-1635	249	8	cell	cell	NOUN
eurjchem-1635	249	9	line	line	NOUN
eurjchem-1635	249	10	(	(	PUNCT
eurjchem-1635	249	11	atcc	atcc	PROPN
eurjchem-1635	249	12	crl‐1730	crl‐1730	PROPN
eurjchem-1635	249	13	)	)	PUNCT
eurjchem-1635	249	14	.	.	PUNCT
eurjchem-1635	250	1	f	f	PROPN
eurjchem-1635	250	2	selectivity	selectivity	NOUN
eurjchem-1635	250	3	index	index	NOUN
eurjchem-1635	250	4	(	(	PUNCT
eurjchem-1635	250	5	si)=	si)=	PROPN
eurjchem-1635	250	6	ic50	ic50	PROPN
eurjchem-1635	250	7	of	of	ADP
eurjchem-1635	250	8	pure	pure	ADJ
eurjchem-1635	250	9	compound	compound	NOUN
eurjchem-1635	250	10	in	in	ADP
eurjchem-1635	250	11	normal	normal	ADJ
eurjchem-1635	250	12	cell	cell	NOUN
eurjchem-1635	250	13	line	line	NOUN
eurjchem-1635	250	14	/	/	SYM
eurjchem-1635	250	15	ic50	ic50	PROPN
eurjchem-1635	250	16	of	of	ADP
eurjchem-1635	250	17	same	same	ADJ
eurjchem-1635	250	18	compound	compound	NOUN
eurjchem-1635	250	19	in	in	ADP
eurjchem-1635	250	20	cancer	cancer	NOUN
eurjchem-1635	250	21	cell	cell	NOUN
eurjchem-1635	250	22	line	line	NOUN
eurjchem-1635	250	23	;	;	PUNCT
eurjchem-1635	250	24	ic50	ic50	PROPN
eurjchem-1635	250	25	:	:	PUNCT
eurjchem-1635	250	26	the	the	DET
eurjchem-1635	250	27	concentration	concentration	NOUN
eurjchem-1635	250	28	required	require	VERB
eurjchem-1635	250	29	to	to	PART
eurjchem-1635	250	30	inhibit	inhibit	VERB
eurjchem-1635	250	31	50	50	NUM
eurjchem-1635	250	32	%	%	NOUN
eurjchem-1635	250	33	of	of	ADP
eurjchem-1635	250	34	cell	cell	NOUN
eurjchem-1635	250	35	population	population	NOUN
eurjchem-1635	250	36	.	.	PUNCT
eurjchem-1635	251	1	in	in	ADP
eurjchem-1635	251	2	entries	entry	NOUN
eurjchem-1635	251	3	6	6	NUM
eurjchem-1635	251	4	and	and	CCONJ
eurjchem-1635	251	5	7	7	NUM
eurjchem-1635	251	6	,	,	PUNCT
eurjchem-1635	251	7	we	we	PRON
eurjchem-1635	251	8	have	have	AUX
eurjchem-1635	251	9	used	use	VERB
eurjchem-1635	251	10	dmap	dmap	NOUN
eurjchem-1635	251	11	as	as	ADP
eurjchem-1635	251	12	an	an	DET
eurjchem-1635	251	13	additive	additive	NOUN
eurjchem-1635	251	14	in	in	ADP
eurjchem-1635	251	15	ratio	ratio	NOUN
eurjchem-1635	251	16	of	of	ADP
eurjchem-1635	251	17	(	(	PUNCT
eurjchem-1635	251	18	for	for	ADP
eurjchem-1635	251	19	entry	entry	NOUN
eurjchem-1635	251	20	6	6	NUM
eurjchem-1635	251	21	,	,	PUNCT
eurjchem-1635	251	22	1	1	NUM
eurjchem-1635	251	23	equiv	equiv	NOUN
eurjchem-1635	251	24	.	.	PUNCT
eurjchem-1635	252	1	2,6	2,6	NUM
eurjchem-1635	252	2	leutidine	leutidine	NOUN
eurjchem-1635	252	3	:	:	PUNCT
eurjchem-1635	252	4	1	1	NUM
eurjchem-1635	252	5	equiv	equiv	NOUN
eurjchem-1635	252	6	.	.	PUNCT
eurjchem-1635	253	1	dmap	dmap	NOUN
eurjchem-1635	253	2	;	;	PUNCT
eurjchem-1635	253	3	and	and	CCONJ
eurjchem-1635	253	4	for	for	ADP
eurjchem-1635	253	5	entry	entry	NOUN
eurjchem-1635	253	6	7	7	NUM
eurjchem-1635	253	7	,	,	PUNCT
eurjchem-1635	253	8	1	1	NUM
eurjchem-1635	253	9	equiv	equiv	NOUN
eurjchem-1635	253	10	.	.	PUNCT
eurjchem-1635	254	1	2,6‐leutidine	2,6‐leutidine	NUM
eurjchem-1635	254	2	:	:	PUNCT
eurjchem-1635	254	3	0.5	0.5	NUM
eurjchem-1635	254	4	equiv	equiv	NOUN
eurjchem-1635	254	5	.	.	PUNCT
eurjchem-1635	255	1	dmap	dmap	NOUN
eurjchem-1635	255	2	)	)	PUNCT
eurjchem-1635	256	1	interes‐	interes‐	VERB
eurjchem-1635	257	1	tingly	tingly	ADV
eurjchem-1635	257	2	yield	yield	NOUN
eurjchem-1635	257	3	is	be	AUX
eurjchem-1635	257	4	increased	increase	VERB
eurjchem-1635	257	5	.	.	PUNCT
eurjchem-1635	258	1	further	far	ADV
eurjchem-1635	258	2	,	,	PUNCT
eurjchem-1635	258	3	we	we	PRON
eurjchem-1635	258	4	have	have	AUX
eurjchem-1635	258	5	modified	modify	VERB
eurjchem-1635	258	6	the	the	DET
eurjchem-1635	258	7	conditions	condition	NOUN
eurjchem-1635	258	8	in	in	ADP
eurjchem-1635	258	9	entry	entry	NOUN
eurjchem-1635	258	10	8	8	NUM
eurjchem-1635	258	11	.	.	PUNCT
eurjchem-1635	259	1	in	in	ADP
eurjchem-1635	259	2	entry	entry	NOUN
eurjchem-1635	259	3	8	8	NUM
eurjchem-1635	259	4	,	,	PUNCT
eurjchem-1635	259	5	we	we	PRON
eurjchem-1635	259	6	have	have	AUX
eurjchem-1635	259	7	used	use	VERB
eurjchem-1635	259	8	2	2	NUM
eurjchem-1635	259	9	equiv	equiv	NOUN
eurjchem-1635	259	10	.	.	PUNCT
eurjchem-1635	260	1	of	of	ADP
eurjchem-1635	260	2	2,6‐	2,6‐	NUM
eurjchem-1635	260	3	lutidine	lutidine	NOUN
eurjchem-1635	260	4	and	and	CCONJ
eurjchem-1635	260	5	0.2	0.2	NUM
eurjchem-1635	260	6	equiv	equiv	NOUN
eurjchem-1635	260	7	.	.	PUNCT
eurjchem-1635	261	1	of	of	ADP
eurjchem-1635	261	2	dmap	dmap	NOUN
eurjchem-1635	261	3	,	,	PUNCT
eurjchem-1635	261	4	the	the	DET
eurjchem-1635	261	5	obtained	obtain	VERB
eurjchem-1635	261	6	yield	yield	NOUN
eurjchem-1635	261	7	was	be	AUX
eurjchem-1635	261	8	85	85	NUM
eurjchem-1635	261	9	%	%	NOUN
eurjchem-1635	261	10	after	after	ADP
eurjchem-1635	261	11	direct	direct	ADJ
eurjchem-1635	261	12	heating	heating	NOUN
eurjchem-1635	261	13	the	the	DET
eurjchem-1635	261	14	reaction	reaction	NOUN
eurjchem-1635	261	15	mixture	mixture	NOUN
eurjchem-1635	261	16	at	at	ADP
eurjchem-1635	261	17	80	80	NUM
eurjchem-1635	261	18	°	°	NUM
eurjchem-1635	261	19	c	c	NOUN
eurjchem-1635	261	20	for	for	ADP
eurjchem-1635	261	21	1	1	NUM
eurjchem-1635	261	22	h	h	NOUN
eurjchem-1635	261	23	by	by	ADP
eurjchem-1635	261	24	using	use	VERB
eurjchem-1635	261	25	chilled	chill	VERB
eurjchem-1635	261	26	water	water	NOUN
eurjchem-1635	261	27	circulating	circulate	VERB
eurjchem-1635	261	28	condenser	condenser	NOUN
eurjchem-1635	261	29	we	we	PRON
eurjchem-1635	261	30	obtain	obtain	AUX
eurjchem-1635	261	31	yield	yield	VERB
eurjchem-1635	261	32	85	85	NUM
eurjchem-1635	261	33	%	%	NOUN
eurjchem-1635	261	34	in	in	ADP
eurjchem-1635	261	35	scheme	scheme	NOUN
eurjchem-1635	261	36	1	1	NUM
eurjchem-1635	261	37	.	.	PUNCT
eurjchem-1635	262	1	in	in	ADP
eurjchem-1635	262	2	scheme	scheme	NOUN
eurjchem-1635	262	3	2	2	NUM
eurjchem-1635	262	4	,	,	PUNCT
eurjchem-1635	262	5	for	for	ADP
eurjchem-1635	262	6	step	step	NOUN
eurjchem-1635	262	7	b	b	NOUN
eurjchem-1635	262	8	,	,	PUNCT
eurjchem-1635	262	9	all	all	DET
eurjchem-1635	262	10	the	the	DET
eurjchem-1635	262	11	conditions	condition	NOUN
eurjchem-1635	262	12	mentioned	mention	VERB
eurjchem-1635	262	13	in	in	ADP
eurjchem-1635	262	14	table	table	NOUN
eurjchem-1635	262	15	2	2	NUM
eurjchem-1635	262	16	are	be	AUX
eurjchem-1635	262	17	failed	fail	VERB
eurjchem-1635	262	18	to	to	PART
eurjchem-1635	262	19	give	give	VERB
eurjchem-1635	262	20	good	good	ADJ
eurjchem-1635	262	21	yields	yield	NOUN
eurjchem-1635	262	22	so	so	ADV
eurjchem-1635	262	23	need	need	VERB
eurjchem-1635	262	24	to	to	PART
eurjchem-1635	262	25	modify	modify	VERB
eurjchem-1635	262	26	the	the	DET
eurjchem-1635	262	27	condition	condition	NOUN
eurjchem-1635	262	28	for	for	ADP
eurjchem-1635	262	29	synthesis	synthesis	NOUN
eurjchem-1635	262	30	of	of	ADP
eurjchem-1635	262	31	compound	compound	NOUN
eurjchem-1635	262	32	6	6	NUM
eurjchem-1635	262	33	.	.	PUNCT
eurjchem-1635	263	1	we	we	PRON
eurjchem-1635	263	2	have	have	VERB
eurjchem-1635	263	3	modified	modify	VERB
eurjchem-1635	263	4	conditions	condition	NOUN
eurjchem-1635	263	5	(	(	PUNCT
eurjchem-1635	263	6	step	step	NOUN
eurjchem-1635	263	7	(	(	PUNCT
eurjchem-1635	263	8	b	b	NOUN
eurjchem-1635	263	9	)	)	PUNCT
eurjchem-1635	263	10	,	,	PUNCT
eurjchem-1635	263	11	scheme	scheme	NOUN
eurjchem-1635	263	12	2	2	NUM
eurjchem-1635	263	13	)	)	PUNCT
eurjchem-1635	263	14	for	for	ADP
eurjchem-1635	263	15	phenylmethanethiol	phenylmethanethiol	NOUN
eurjchem-1635	263	16	by	by	ADP
eurjchem-1635	263	17	changing	change	VERB
eurjchem-1635	263	18	base	base	NOUN
eurjchem-1635	263	19	as	as	ADP
eurjchem-1635	263	20	sodium	sodium	NOUN
eurjchem-1635	263	21	hydroxide	hydroxide	NOUN
eurjchem-1635	263	22	in	in	ADP
eurjchem-1635	263	23	thf	thf	NOUN
eurjchem-1635	263	24	and	and	CCONJ
eurjchem-1635	263	25	heating	heating	NOUN
eurjchem-1635	263	26	at	at	ADP
eurjchem-1635	263	27	80	80	NUM
eurjchem-1635	263	28	°	°	NUM
eurjchem-1635	263	29	c	c	NOUN
eurjchem-1635	263	30	for	for	ADP
eurjchem-1635	263	31	1	1	NUM
eurjchem-1635	263	32	h	h	NOUN
eurjchem-1635	263	33	to	to	PART
eurjchem-1635	263	34	obtain	obtain	VERB
eurjchem-1635	263	35	the	the	DET
eurjchem-1635	263	36	desired	desire	VERB
eurjchem-1635	263	37	product	product	NOUN
eurjchem-1635	263	38	in	in	ADP
eurjchem-1635	263	39	87	87	NUM
eurjchem-1635	263	40	%	%	NOUN
eurjchem-1635	263	41	yield	yield	NOUN
eurjchem-1635	263	42	which	which	PRON
eurjchem-1635	263	43	is	be	AUX
eurjchem-1635	263	44	used	use	VERB
eurjchem-1635	263	45	further	far	ADV
eurjchem-1635	263	46	for	for	ADP
eurjchem-1635	263	47	sulfonamide	sulfonamide	NOUN
eurjchem-1635	263	48	coupling	coupling	NOUN
eurjchem-1635	263	49	reaction	reaction	NOUN
eurjchem-1635	263	50	.	.	PUNCT
eurjchem-1635	264	1	we	we	PRON
eurjchem-1635	264	2	have	have	AUX
eurjchem-1635	264	3	modified	modify	VERB
eurjchem-1635	264	4	the	the	DET
eurjchem-1635	264	5	base	base	NOUN
eurjchem-1635	264	6	and	and	CCONJ
eurjchem-1635	264	7	we	we	PRON
eurjchem-1635	264	8	got	get	VERB
eurjchem-1635	264	9	the	the	DET
eurjchem-1635	264	10	yield	yield	NOUN
eurjchem-1635	264	11	87	87	NUM
eurjchem-1635	264	12	%	%	NOUN
eurjchem-1635	264	13	without	without	ADP
eurjchem-1635	264	14	purification	purification	NOUN
eurjchem-1635	264	15	which	which	PRON
eurjchem-1635	264	16	is	be	AUX
eurjchem-1635	264	17	used	use	VERB
eurjchem-1635	264	18	further	far	ADV
eurjchem-1635	264	19	for	for	ADP
eurjchem-1635	264	20	synthesis	synthesis	NOUN
eurjchem-1635	264	21	of	of	ADP
eurjchem-1635	264	22	compounds	compound	NOUN
eurjchem-1635	264	23	7a‐e	7a‐e	PROPN
eurjchem-1635	264	24	.	.	PUNCT
eurjchem-1635	265	1	during	during	ADP
eurjchem-1635	265	2	synthesis	synthesis	NOUN
eurjchem-1635	265	3	of	of	ADP
eurjchem-1635	265	4	compound	compound	NOUN
eurjchem-1635	265	5	6	6	NUM
eurjchem-1635	265	6	by	by	ADP
eurjchem-1635	265	7	using	use	VERB
eurjchem-1635	265	8	table	table	NOUN
eurjchem-1635	265	9	2	2	NUM
eurjchem-1635	265	10	conditions	condition	NOUN
eurjchem-1635	265	11	,	,	PUNCT
eurjchem-1635	265	12	we	we	PRON
eurjchem-1635	265	13	got	get	VERB
eurjchem-1635	265	14	sluggish	sluggish	ADJ
eurjchem-1635	265	15	reaction	reaction	NOUN
eurjchem-1635	265	16	mixture	mixture	NOUN
eurjchem-1635	265	17	which	which	PRON
eurjchem-1635	265	18	is	be	AUX
eurjchem-1635	265	19	difficult	difficult	ADJ
eurjchem-1635	265	20	to	to	PART
eurjchem-1635	265	21	purify	purify	VERB
eurjchem-1635	265	22	multiple	multiple	ADJ
eurjchem-1635	265	23	spots	spot	NOUN
eurjchem-1635	265	24	on	on	ADP
eurjchem-1635	265	25	tlc	tlc	NOUN
eurjchem-1635	265	26	and	and	CCONJ
eurjchem-1635	265	27	lc‐ms	lc‐ms	NOUN
eurjchem-1635	265	28	showing	show	VERB
eurjchem-1635	265	29	multiple	multiple	ADJ
eurjchem-1635	265	30	unidentified	unidentified	ADJ
eurjchem-1635	265	31	masses	masse	NOUN
eurjchem-1635	265	32	so	so	SCONJ
eurjchem-1635	265	33	we	we	PRON
eurjchem-1635	265	34	modified	modify	VERB
eurjchem-1635	265	35	the	the	DET
eurjchem-1635	265	36	conditions	condition	NOUN
eurjchem-1635	265	37	b	b	NOUN
eurjchem-1635	265	38	in	in	ADP
eurjchem-1635	265	39	scheme	scheme	NOUN
eurjchem-1635	265	40	2	2	NUM
eurjchem-1635	265	41	for	for	ADP
eurjchem-1635	265	42	synthesis	synthesis	NOUN
eurjchem-1635	265	43	of	of	ADP
eurjchem-1635	265	44	compound	compound	NOUN
eurjchem-1635	265	45	6	6	NUM
eurjchem-1635	265	46	.	.	PUNCT
eurjchem-1635	266	1	for	for	ADP
eurjchem-1635	266	2	step	step	NOUN
eurjchem-1635	266	3	(	(	PUNCT
eurjchem-1635	266	4	c	c	NOUN
eurjchem-1635	266	5	)	)	PUNCT
eurjchem-1635	266	6	(	(	PUNCT
eurjchem-1635	266	7	scheme	scheme	NOUN
eurjchem-1635	266	8	1	1	NUM
eurjchem-1635	266	9	)	)	PUNCT
eurjchem-1635	266	10	,	,	PUNCT
eurjchem-1635	266	11	we	we	PRON
eurjchem-1635	266	12	have	have	AUX
eurjchem-1635	266	13	used	use	VERB
eurjchem-1635	266	14	raney	raney	PROPN
eurjchem-1635	266	15	ni	ni	PROPN
eurjchem-1635	266	16	with	with	ADP
eurjchem-1635	266	17	hydrogen	hydrogen	NOUN
eurjchem-1635	266	18	gas	gas	NOUN
eurjchem-1635	266	19	pressure	pressure	NOUN
eurjchem-1635	266	20	of	of	ADP
eurjchem-1635	266	21	60	60	NUM
eurjchem-1635	266	22	psi	psi	NOUN
eurjchem-1635	266	23	in	in	ADP
eurjchem-1635	266	24	parr	parr	ADJ
eurjchem-1635	266	25	shaker	shaker	NOUN
eurjchem-1635	266	26	in	in	ADP
eurjchem-1635	266	27	saturated	saturate	VERB
eurjchem-1635	266	28	methanolic	methanolic	NOUN
eurjchem-1635	266	29	ammonia	ammonia	NOUN
eurjchem-1635	266	30	for	for	ADP
eurjchem-1635	266	31	3	3	NUM
eurjchem-1635	266	32	h	h	NOUN
eurjchem-1635	266	33	at	at	ADP
eurjchem-1635	266	34	room	room	NOUN
eurjchem-1635	266	35	temperature	temperature	NOUN
eurjchem-1635	266	36	;	;	PUNCT
eurjchem-1635	266	37	it	it	PRON
eurjchem-1635	266	38	gives	give	VERB
eurjchem-1635	266	39	the	the	DET
eurjchem-1635	266	40	best	good	ADJ
eurjchem-1635	266	41	results	result	NOUN
eurjchem-1635	266	42	and	and	CCONJ
eurjchem-1635	266	43	yield	yield	NOUN
eurjchem-1635	266	44	obtained	obtain	VERB
eurjchem-1635	266	45	is	be	AUX
eurjchem-1635	266	46	85	85	NUM
eurjchem-1635	266	47	%	%	NOUN
eurjchem-1635	266	48	.	.	PUNCT
eurjchem-1635	267	1	for	for	ADP
eurjchem-1635	267	2	step	step	NOUN
eurjchem-1635	267	3	(	(	PUNCT
eurjchem-1635	267	4	d	d	NOUN
eurjchem-1635	267	5	)	)	PUNCT
eurjchem-1635	267	6	(	(	PUNCT
eurjchem-1635	267	7	scheme	scheme	NOUN
eurjchem-1635	267	8	1	1	NUM
eurjchem-1635	267	9	and	and	CCONJ
eurjchem-1635	267	10	2	2	NUM
eurjchem-1635	267	11	)	)	PUNCT
eurjchem-1635	267	12	,	,	PUNCT
eurjchem-1635	267	13	we	we	PRON
eurjchem-1635	267	14	have	have	AUX
eurjchem-1635	267	15	used	use	VERB
eurjchem-1635	267	16	1:1	1:1	NUM
eurjchem-1635	267	17	mixture	mixture	NOUN
eurjchem-1635	267	18	of	of	ADP
eurjchem-1635	267	19	dcm	dcm	NOUN
eurjchem-1635	267	20	and	and	CCONJ
eurjchem-1635	267	21	pyridine	pyridine	NOUN
eurjchem-1635	267	22	as	as	ADP
eurjchem-1635	267	23	a	a	DET
eurjchem-1635	267	24	solvent	solvent	NOUN
eurjchem-1635	267	25	and	and	CCONJ
eurjchem-1635	267	26	base	base	NOUN
eurjchem-1635	267	27	to	to	PART
eurjchem-1635	267	28	get	get	VERB
eurjchem-1635	267	29	yields	yield	NOUN
eurjchem-1635	267	30	ranging	range	VERB
eurjchem-1635	267	31	from	from	ADP
eurjchem-1635	267	32	80‐95	80‐95	NUM
eurjchem-1635	267	33	%	%	NOUN
eurjchem-1635	267	34	for	for	ADP
eurjchem-1635	267	35	all	all	DET
eurjchem-1635	267	36	the	the	DET
eurjchem-1635	267	37	compounds	compound	NOUN
eurjchem-1635	267	38	4a‐e	4a‐e	NOUN
eurjchem-1635	267	39	and	and	CCONJ
eurjchem-1635	267	40	7a‐e	7a‐e	PROPN
eurjchem-1635	267	41	.	.	PUNCT
eurjchem-1635	268	1	3.2	3.2	NUM
eurjchem-1635	268	2	.	.	PUNCT
eurjchem-1635	268	3	anticancer	anticancer	NOUN
eurjchem-1635	268	4	activity	activity	NOUN
eurjchem-1635	268	5	all	all	DET
eurjchem-1635	268	6	the	the	DET
eurjchem-1635	268	7	newly	newly	ADV
eurjchem-1635	268	8	synthesized	synthesize	VERB
eurjchem-1635	268	9	compounds	compound	NOUN
eurjchem-1635	268	10	4a‐e	4a‐e	NOUN
eurjchem-1635	268	11	and	and	CCONJ
eurjchem-1635	268	12	7a‐e	7a‐e	PROPN
eurjchem-1635	268	13	were	be	AUX
eurjchem-1635	268	14	evaluated	evaluate	VERB
eurjchem-1635	268	15	for	for	ADP
eurjchem-1635	268	16	their	their	PRON
eurjchem-1635	268	17	antiproliferative	antiproliferative	ADJ
eurjchem-1635	268	18	activities	activity	NOUN
eurjchem-1635	268	19	against	against	ADP
eurjchem-1635	268	20	a	a	DET
eurjchem-1635	268	21	panel	panel	NOUN
eurjchem-1635	268	22	of	of	ADP
eurjchem-1635	268	23	four	four	NUM
eurjchem-1635	268	24	different	different	ADJ
eurjchem-1635	268	25	human	human	ADJ
eurjchem-1635	268	26	cancer	cancer	NOUN
eurjchem-1635	268	27	cell	cell	NOUN
eurjchem-1635	268	28	lines	line	NOUN
eurjchem-1635	268	29	.	.	PUNCT
eurjchem-1635	269	1	the	the	DET
eurjchem-1635	269	2	ic50	ic50	PROPN
eurjchem-1635	269	3	for	for	ADP
eurjchem-1635	269	4	each	each	DET
eurjchem-1635	269	5	synthesized	synthesize	VERB
eurjchem-1635	269	6	compounds	compound	NOUN
eurjchem-1635	269	7	are	be	AUX
eurjchem-1635	269	8	calculated	calculate	VERB
eurjchem-1635	269	9	with	with	ADP
eurjchem-1635	269	10	respect	respect	NOUN
eurjchem-1635	269	11	to	to	ADP
eurjchem-1635	269	12	one	one	NUM
eurjchem-1635	269	13	human	human	ADJ
eurjchem-1635	269	14	normal	normal	ADJ
eurjchem-1635	269	15	cell	cell	NOUN
eurjchem-1635	269	16	line	line	NOUN
eurjchem-1635	269	17	human	human	ADJ
eurjchem-1635	269	18	umbilical	umbilical	ADJ
eurjchem-1635	269	19	vein	vein	ADJ
eurjchem-1635	269	20	endothelial	endothelial	ADJ
eurjchem-1635	269	21	cell	cell	NOUN
eurjchem-1635	269	22	line	line	NOUN
eurjchem-1635	269	23	(	(	PUNCT
eurjchem-1635	269	24	atcc	atcc	PROPN
eurjchem-1635	269	25	crl‐1730	crl‐1730	PROPN
eurjchem-1635	269	26	)	)	PUNCT
eurjchem-1635	269	27	and	and	CCONJ
eurjchem-1635	269	28	results	result	NOUN
eurjchem-1635	269	29	are	be	AUX
eurjchem-1635	269	30	summarized	summarize	VERB
eurjchem-1635	269	31	in	in	ADP
eurjchem-1635	269	32	table	table	NOUN
eurjchem-1635	269	33	3	3	NUM
eurjchem-1635	269	34	.	.	PUNCT
eurjchem-1635	270	1	these	these	DET
eurjchem-1635	270	2	values	value	NOUN
eurjchem-1635	270	3	represent	represent	VERB
eurjchem-1635	270	4	the	the	DET
eurjchem-1635	270	5	concentration	concentration	NOUN
eurjchem-1635	270	6	required	require	VERB
eurjchem-1635	270	7	to	to	PART
eurjchem-1635	270	8	inhibit	inhibit	VERB
eurjchem-1635	270	9	50	50	NUM
eurjchem-1635	270	10	%	%	NOUN
eurjchem-1635	270	11	cell	cell	NOUN
eurjchem-1635	270	12	population	population	NOUN
eurjchem-1635	270	13	compared	compare	VERB
eurjchem-1635	270	14	with	with	ADP
eurjchem-1635	270	15	the	the	DET
eurjchem-1635	270	16	control	control	NOUN
eurjchem-1635	270	17	cells	cell	NOUN
eurjchem-1635	270	18	treated	treat	VERB
eurjchem-1635	270	19	with	with	ADP
eurjchem-1635	270	20	dmso	dmso	NOUN
eurjchem-1635	270	21	and	and	CCONJ
eurjchem-1635	270	22	positive	positive	ADJ
eurjchem-1635	270	23	control	control	NOUN
eurjchem-1635	270	24	5‐fluorouracil	5‐fluorouracil	PROPN
eurjchem-1635	270	25	under	under	ADP
eurjchem-1635	270	26	similar	similar	ADJ
eurjchem-1635	270	27	conditions	condition	NOUN
eurjchem-1635	270	28	.	.	PUNCT
eurjchem-1635	271	1	from	from	ADP
eurjchem-1635	271	2	compounds	compound	NOUN
eurjchem-1635	271	3	4a‐4e	4a‐4e	NOUN
eurjchem-1635	271	4	,	,	PUNCT
eurjchem-1635	271	5	the	the	DET
eurjchem-1635	271	6	ic50	ic50	PROPN
eurjchem-1635	271	7	value	value	NOUN
eurjchem-1635	271	8	ranges	range	VERB
eurjchem-1635	271	9	from	from	ADP
eurjchem-1635	271	10	10.65	10.65	NUM
eurjchem-1635	271	11	to	to	ADP
eurjchem-1635	271	12	33.81	33.81	NUM
eurjchem-1635	271	13	µm	µm	ADP
eurjchem-1635	271	14	all	all	DET
eurjchem-1635	271	15	four	four	NUM
eurjchem-1635	271	16	cell	cell	NOUN
eurjchem-1635	271	17	lines	line	NOUN
eurjchem-1635	271	18	.	.	PUNCT
eurjchem-1635	272	1	for	for	ADP
eurjchem-1635	272	2	cell	cell	NOUN
eurjchem-1635	272	3	line	line	NOUN
eurjchem-1635	272	4	a‐549	a‐549	NOUN
eurjchem-1635	272	5	compound	compound	NOUN
eurjchem-1635	272	6	4c	4c	NOUN
eurjchem-1635	272	7	is	be	AUX
eurjchem-1635	272	8	most	most	ADV
eurjchem-1635	272	9	active	active	ADJ
eurjchem-1635	272	10	with	with	ADP
eurjchem-1635	272	11	ic50	ic50	PROPN
eurjchem-1635	272	12	value	value	NOUN
eurjchem-1635	272	13	of	of	ADP
eurjchem-1635	272	14	10.65	10.65	NUM
eurjchem-1635	272	15	µm	µm	NOUN
eurjchem-1635	272	16	and	and	CCONJ
eurjchem-1635	272	17	compound	compound	NOUN
eurjchem-1635	272	18	4d	4d	NOUN
eurjchem-1635	272	19	is	be	AUX
eurjchem-1635	272	20	also	also	ADV
eurjchem-1635	272	21	active	active	ADJ
eurjchem-1635	272	22	with	with	ADP
eurjchem-1635	272	23	ic50	ic50	PROPN
eurjchem-1635	272	24	value	value	NOUN
eurjchem-1635	272	25	of	of	ADP
eurjchem-1635	272	26	10.81	10.81	NUM
eurjchem-1635	272	27	µm	µm	NOUN
eurjchem-1635	272	28	.	.	PUNCT
eurjchem-1635	273	1	compound	compound	NOUN
eurjchem-1635	273	2	4b	4b	PROPN
eurjchem-1635	273	3	is	be	AUX
eurjchem-1635	273	4	very	very	ADV
eurjchem-1635	273	5	less	less	ADV
eurjchem-1635	273	6	active	active	ADJ
eurjchem-1635	273	7	with	with	ADP
eurjchem-1635	273	8	ic50	ic50	PROPN
eurjchem-1635	273	9	value	value	NOUN
eurjchem-1635	273	10	of	of	ADP
eurjchem-1635	273	11	33.81	33.81	NUM
eurjchem-1635	273	12	µm	µm	NOUN
eurjchem-1635	273	13	.	.	PUNCT
eurjchem-1635	274	1	similar	similar	ADJ
eurjchem-1635	274	2	results	result	NOUN
eurjchem-1635	274	3	are	be	AUX
eurjchem-1635	274	4	obtained	obtain	VERB
eurjchem-1635	274	5	with	with	ADP
eurjchem-1635	274	6	remaining	remain	VERB
eurjchem-1635	274	7	cell	cell	NOUN
eurjchem-1635	274	8	lines	line	NOUN
eurjchem-1635	274	9	.	.	PUNCT
eurjchem-1635	275	1	compound	compound	NOUN
eurjchem-1635	275	2	4d	4d	NOUN
eurjchem-1635	275	3	having	have	VERB
eurjchem-1635	275	4	ic50	ic50	PROPN
eurjchem-1635	275	5	values	value	NOUN
eurjchem-1635	275	6	of	of	ADP
eurjchem-1635	275	7	10.79	10.79	NUM
eurjchem-1635	275	8	,	,	PUNCT
eurjchem-1635	275	9	12.86	12.86	NUM
eurjchem-1635	275	10	and	and	CCONJ
eurjchem-1635	275	11	10.82	10.82	NUM
eurjchem-1635	275	12	µm	µm	NOUN
eurjchem-1635	275	13	in	in	ADP
eurjchem-1635	275	14	hela	hela	PROPN
eurjchem-1635	275	15	,	,	PUNCT
eurjchem-1635	275	16	mcf‐7	mcf‐7	PROPN
eurjchem-1635	275	17	and	and	CCONJ
eurjchem-1635	275	18	du‐145	du‐145	NOUN
eurjchem-1635	275	19	cell	cell	NOUN
eurjchem-1635	275	20	lines	line	NOUN
eurjchem-1635	275	21	,	,	PUNCT
eurjchem-1635	275	22	respectively	respectively	ADV
eurjchem-1635	275	23	.	.	PUNCT
eurjchem-1635	276	1	the	the	DET
eurjchem-1635	276	2	compound	compound	NOUN
eurjchem-1635	276	3	4c	4c	NOUN
eurjchem-1635	276	4	is	be	AUX
eurjchem-1635	276	5	active	active	ADJ
eurjchem-1635	276	6	in	in	ADP
eurjchem-1635	276	7	a‐549	a‐549	NOUN
eurjchem-1635	276	8	only	only	ADV
eurjchem-1635	276	9	,	,	PUNCT
eurjchem-1635	276	10	it	it	PRON
eurjchem-1635	276	11	is	be	AUX
eurjchem-1635	276	12	less	less	ADV
eurjchem-1635	276	13	active	active	ADJ
eurjchem-1635	276	14	in	in	ADP
eurjchem-1635	276	15	hela	hela	PROPN
eurjchem-1635	276	16	,	,	PUNCT
eurjchem-1635	276	17	mcf‐7	mcf‐7	PROPN
eurjchem-1635	276	18	and	and	CCONJ
eurjchem-1635	276	19	du‐145	du‐145	NOUN
eurjchem-1635	276	20	cell	cell	NOUN
eurjchem-1635	276	21	lines	line	NOUN
eurjchem-1635	276	22	with	with	ADP
eurjchem-1635	276	23	ic50	ic50	PROPN
eurjchem-1635	276	24	values	value	NOUN
eurjchem-1635	276	25	of	of	ADP
eurjchem-1635	276	26	28.32	28.32	NUM
eurjchem-1635	276	27	,	,	PUNCT
eurjchem-1635	276	28	27.32	27.32	NUM
eurjchem-1635	276	29	and	and	CCONJ
eurjchem-1635	276	30	20.73	20.73	NUM
eurjchem-1635	276	31	µm	µm	NOUN
eurjchem-1635	276	32	,	,	PUNCT
eurjchem-1635	276	33	respectively	respectively	ADV
eurjchem-1635	276	34	.	.	PUNCT
eurjchem-1635	277	1	the	the	DET
eurjchem-1635	277	2	compounds	compound	NOUN
eurjchem-1635	277	3	7a‐e	7a‐e	VERB
eurjchem-1635	277	4	the	the	DET
eurjchem-1635	277	5	ic50	ic50	PROPN
eurjchem-1635	277	6	value	value	NOUN
eurjchem-1635	277	7	ranges	range	VERB
eurjchem-1635	277	8	from	from	ADP
eurjchem-1635	277	9	10.78	10.78	NUM
eurjchem-1635	277	10	to	to	ADP
eurjchem-1635	277	11	33.82	33.82	NUM
eurjchem-1635	277	12	µm	µm	NOUN
eurjchem-1635	277	13	.	.	PUNCT
eurjchem-1635	278	1	for	for	ADP
eurjchem-1635	278	2	cell	cell	NOUN
eurjchem-1635	278	3	line	line	NOUN
eurjchem-1635	278	4	a‐549	a‐549	NOUN
eurjchem-1635	278	5	,	,	PUNCT
eurjchem-1635	278	6	compound	compound	NOUN
eurjchem-1635	278	7	7d	7d	NOUN
eurjchem-1635	278	8	and	and	CCONJ
eurjchem-1635	278	9	7c	7c	NUM
eurjchem-1635	278	10	are	be	AUX
eurjchem-1635	278	11	active	active	ADJ
eurjchem-1635	278	12	with	with	ADP
eurjchem-1635	278	13	ic50	ic50	PROPN
eurjchem-1635	278	14	value	value	NOUN
eurjchem-1635	278	15	of	of	ADP
eurjchem-1635	278	16	10.82	10.82	NUM
eurjchem-1635	278	17	and10.78	and10.78	NOUN
eurjchem-1635	278	18	µm	µm	NOUN
eurjchem-1635	278	19	,	,	PUNCT
eurjchem-1635	278	20	respectively	respectively	ADV
eurjchem-1635	278	21	.	.	PUNCT
eurjchem-1635	279	1	compound	compound	NOUN
eurjchem-1635	279	2	7b	7b	PROPN
eurjchem-1635	279	3	is	be	AUX
eurjchem-1635	279	4	less	less	ADV
eurjchem-1635	279	5	active	active	ADJ
eurjchem-1635	279	6	with	with	ADP
eurjchem-1635	279	7	ic50	ic50	PROPN
eurjchem-1635	279	8	value	value	NOUN
eurjchem-1635	279	9	of	of	ADP
eurjchem-1635	279	10	33.82	33.82	NUM
eurjchem-1635	279	11	µm	µm	NOUN
eurjchem-1635	279	12	.	.	PUNCT
eurjchem-1635	280	1	similar	similar	ADJ
eurjchem-1635	280	2	results	result	NOUN
eurjchem-1635	280	3	are	be	AUX
eurjchem-1635	280	4	obtained	obtain	VERB
eurjchem-1635	280	5	with	with	ADP
eurjchem-1635	280	6	remaining	remain	VERB
eurjchem-1635	280	7	cell	cell	NOUN
eurjchem-1635	280	8	lines	line	NOUN
eurjchem-1635	280	9	.	.	PUNCT
eurjchem-1635	281	1	compound	compound	NOUN
eurjchem-1635	281	2	7d	7d	PROPN
eurjchem-1635	281	3	having	have	VERB
eurjchem-1635	281	4	ic50	ic50	PROPN
eurjchem-1635	281	5	values	value	NOUN
eurjchem-1635	281	6	of	of	ADP
eurjchem-1635	281	7	10.99	10.99	NUM
eurjchem-1635	281	8	,	,	PUNCT
eurjchem-1635	281	9	12.36	12.36	NUM
eurjchem-1635	281	10	and	and	CCONJ
eurjchem-1635	281	11	19.52	19.52	NUM
eurjchem-1635	281	12	µm	µm	NOUN
eurjchem-1635	281	13	in	in	ADP
eurjchem-1635	281	14	hela	hela	PROPN
eurjchem-1635	281	15	,	,	PUNCT
eurjchem-1635	281	16	mcf‐7	mcf‐7	PROPN
eurjchem-1635	281	17	and	and	CCONJ
eurjchem-1635	281	18	du‐145	du‐145	NOUN
eurjchem-1635	281	19	cell	cell	NOUN
eurjchem-1635	281	20	lines	line	NOUN
eurjchem-1635	281	21	,	,	PUNCT
eurjchem-1635	281	22	respectively	respectively	ADV
eurjchem-1635	281	23	.	.	PUNCT
eurjchem-1635	282	1	the	the	DET
eurjchem-1635	282	2	compound	compound	NOUN
eurjchem-1635	282	3	7c	7c	PROPN
eurjchem-1635	282	4	is	be	AUX
eurjchem-1635	282	5	active	active	ADJ
eurjchem-1635	282	6	in	in	ADP
eurjchem-1635	282	7	a‐549	a‐549	NOUN
eurjchem-1635	282	8	and	and	CCONJ
eurjchem-1635	282	9	also	also	ADV
eurjchem-1635	282	10	hela	hela	ADJ
eurjchem-1635	282	11	,	,	PUNCT
eurjchem-1635	282	12	mcf‐7	mcf‐7	PROPN
eurjchem-1635	282	13	and	and	CCONJ
eurjchem-1635	282	14	du‐145	du‐145	NOUN
eurjchem-1635	282	15	cell	cell	NOUN
eurjchem-1635	282	16	lines	line	NOUN
eurjchem-1635	282	17	with	with	ADP
eurjchem-1635	282	18	ic50	ic50	PROPN
eurjchem-1635	282	19	values	value	NOUN
eurjchem-1635	282	20	of	of	ADP
eurjchem-1635	282	21	10.78	10.78	NUM
eurjchem-1635	282	22	,	,	PUNCT
eurjchem-1635	282	23	13.82	13.82	NUM
eurjchem-1635	282	24	and	and	CCONJ
eurjchem-1635	282	25	14.72	14.72	NUM
eurjchem-1635	282	26	µm	µm	NOUN
eurjchem-1635	282	27	,	,	PUNCT
eurjchem-1635	282	28	respectively	respectively	ADV
eurjchem-1635	282	29	.	.	PUNCT
eurjchem-1635	283	1	in	in	ADP
eurjchem-1635	283	2	all	all	DET
eurjchem-1635	283	3	the	the	DET
eurjchem-1635	283	4	four	four	NUM
eurjchem-1635	283	5	cell	cell	NOUN
eurjchem-1635	283	6	lines	line	NOUN
eurjchem-1635	283	7	the	the	DET
eurjchem-1635	283	8	compounds	compound	NOUN
eurjchem-1635	283	9	having	have	VERB
eurjchem-1635	283	10	phenyl	phenyl	NOUN
eurjchem-1635	283	11	sulfonamide	sulfonamide	NOUN
eurjchem-1635	283	12	ring	ring	NOUN
eurjchem-1635	283	13	(	(	PUNCT
eurjchem-1635	283	14	compound	compound	NOUN
eurjchem-1635	283	15	4a	4a	NOUN
eurjchem-1635	283	16	and	and	CCONJ
eurjchem-1635	283	17	7a	7a	NUM
eurjchem-1635	283	18	)	)	PUNCT
eurjchem-1635	283	19	are	be	AUX
eurjchem-1635	283	20	moderately	moderately	ADV
eurjchem-1635	283	21	active	active	ADJ
eurjchem-1635	283	22	with	with	ADP
eurjchem-1635	283	23	ic50	ic50	PROPN
eurjchem-1635	283	24	values	value	NOUN
eurjchem-1635	283	25	from	from	ADP
eurjchem-1635	283	26	22.72	22.72	NUM
eurjchem-1635	283	27	to	to	ADP
eurjchem-1635	283	28	28.86	28.86	NUM
eurjchem-1635	283	29	µm	µm	NOUN
eurjchem-1635	283	30	,	,	PUNCT
eurjchem-1635	283	31	respectively	respectively	ADV
eurjchem-1635	283	32	.	.	PUNCT
eurjchem-1635	284	1	compounds	compound	NOUN
eurjchem-1635	284	2	having	have	VERB
eurjchem-1635	284	3	para‐methyl	para‐methyl	NOUN
eurjchem-1635	284	4	phenyl	phenyl	NOUN
eurjchem-1635	284	5	sulfonamide	sulfonamide	NOUN
eurjchem-1635	284	6	ring	ring	NOUN
eurjchem-1635	284	7	(	(	PUNCT
eurjchem-1635	284	8	compound	compound	VERB
eurjchem-1635	284	9	4b	4b	PROPN
eurjchem-1635	284	10	and	and	CCONJ
eurjchem-1635	284	11	7b	7b	NOUN
eurjchem-1635	284	12	)	)	PUNCT
eurjchem-1635	284	13	are	be	AUX
eurjchem-1635	284	14	most	most	ADV
eurjchem-1635	284	15	inactive	inactive	ADJ
eurjchem-1635	284	16	with	with	ADP
eurjchem-1635	284	17	ic50	ic50	PROPN
eurjchem-1635	284	18	value	value	NOUN
eurjchem-1635	284	19	20.36	20.36	NUM
eurjchem-1635	284	20	to	to	ADP
eurjchem-1635	284	21	33.82	33.82	NUM
eurjchem-1635	284	22	µm	µm	NOUN
eurjchem-1635	284	23	,	,	PUNCT
eurjchem-1635	284	24	respectively	respectively	ADV
eurjchem-1635	284	25	.	.	PUNCT
eurjchem-1635	285	1	the	the	DET
eurjchem-1635	285	2	compound	compound	NOUN
eurjchem-1635	285	3	having	have	VERB
eurjchem-1635	285	4	only	only	ADV
eurjchem-1635	285	5	methyl	methyl	NOUN
eurjchem-1635	285	6	sulfonamide	sulfonamide	NOUN
eurjchem-1635	285	7	ring	ring	NOUN
eurjchem-1635	285	8	(	(	PUNCT
eurjchem-1635	285	9	compound	compound	NOUN
eurjchem-1635	285	10	4e	4e	NOUN
eurjchem-1635	285	11	and	and	CCONJ
eurjchem-1635	285	12	7e	7e	NUM
eurjchem-1635	285	13	)	)	PUNCT
eurjchem-1635	285	14	is	be	AUX
eurjchem-1635	285	15	having	have	VERB
eurjchem-1635	285	16	moderate	moderate	ADJ
eurjchem-1635	285	17	ic50	ic50	PROPN
eurjchem-1635	285	18	values	value	NOUN
eurjchem-1635	285	19	from	from	ADP
eurjchem-1635	285	20	14.38	14.38	NUM
eurjchem-1635	285	21	to	to	ADP
eurjchem-1635	285	22	23.86	23.86	NUM
eurjchem-1635	285	23	µm	µm	NOUN
eurjchem-1635	285	24	,	,	PUNCT
eurjchem-1635	285	25	respectively	respectively	ADV
eurjchem-1635	285	26	.	.	PUNCT
eurjchem-1635	286	1	the	the	DET
eurjchem-1635	286	2	compound	compound	NOUN
eurjchem-1635	286	3	4e	4e	NOUN
eurjchem-1635	286	4	is	be	AUX
eurjchem-1635	286	5	most	most	ADV
eurjchem-1635	286	6	active	active	ADJ
eurjchem-1635	286	7	in	in	ADP
eurjchem-1635	286	8	hela	hela	PROPN
eurjchem-1635	286	9	cell	cell	NOUN
eurjchem-1635	286	10	line	line	NOUN
eurjchem-1635	286	11	(	(	PUNCT
eurjchem-1635	286	12	atcc	atcc	ADJ
eurjchem-1635	286	13	ccl‐2	ccl‐2	PROPN
eurjchem-1635	286	14	)	)	PUNCT
eurjchem-1635	286	15	with	with	ADP
eurjchem-1635	286	16	ic50	ic50	PROPN
eurjchem-1635	286	17	value	value	NOUN
eurjchem-1635	286	18	of	of	ADP
eurjchem-1635	286	19	14.38	14.38	NUM
eurjchem-1635	286	20	µm	µm	NOUN
eurjchem-1635	286	21	,	,	PUNCT
eurjchem-1635	286	22	compare	compare	VERB
eurjchem-1635	286	23	to	to	ADP
eurjchem-1635	286	24	it	it	PRON
eurjchem-1635	286	25	is	be	AUX
eurjchem-1635	286	26	inactive	inactive	ADJ
eurjchem-1635	286	27	with	with	ADP
eurjchem-1635	286	28	remaining	remain	VERB
eurjchem-1635	286	29	cell	cell	NOUN
eurjchem-1635	286	30	lines	line	NOUN
eurjchem-1635	286	31	.	.	PUNCT
eurjchem-1635	287	1	interestingly	interestingly	ADV
eurjchem-1635	287	2	compounds	compound	VERB
eurjchem-1635	287	3	having	have	VERB
eurjchem-1635	287	4	electron	electron	NOUN
eurjchem-1635	287	5	withdrawing	withdraw	VERB
eurjchem-1635	287	6	group	group	NOUN
eurjchem-1635	287	7	at	at	ADP
eurjchem-1635	287	8	para	para	NOUN
eurjchem-1635	287	9	position	position	NOUN
eurjchem-1635	287	10	of	of	ADP
eurjchem-1635	287	11	aromatic	aromatic	ADJ
eurjchem-1635	287	12	ring	ring	NOUN
eurjchem-1635	287	13	are	be	AUX
eurjchem-1635	287	14	most	most	ADV
eurjchem-1635	287	15	active	active	ADJ
eurjchem-1635	287	16	on	on	ADP
eurjchem-1635	287	17	all	all	DET
eurjchem-1635	287	18	four	four	NUM
eurjchem-1635	287	19	cell	cell	NOUN
eurjchem-1635	287	20	lines	line	NOUN
eurjchem-1635	287	21	and	and	CCONJ
eurjchem-1635	287	22	that	that	PRON
eurjchem-1635	287	23	of	of	ADP
eurjchem-1635	287	24	electron	electron	NOUN
eurjchem-1635	287	25	donating	donate	VERB
eurjchem-1635	287	26	groups	group	NOUN
eurjchem-1635	287	27	are	be	AUX
eurjchem-1635	287	28	less	less	ADV
eurjchem-1635	287	29	active	active	ADJ
eurjchem-1635	287	30	on	on	ADP
eurjchem-1635	287	31	all	all	DET
eurjchem-1635	287	32	cell	cell	NOUN
eurjchem-1635	287	33	lines	line	NOUN
eurjchem-1635	287	34	.	.	PUNCT
eurjchem-1635	288	1	if	if	SCONJ
eurjchem-1635	288	2	we	we	PRON
eurjchem-1635	288	3	replace	replace	VERB
eurjchem-1635	288	4	aromatic	aromatic	ADJ
eurjchem-1635	288	5	ring	ring	NOUN
eurjchem-1635	288	6	with	with	ADP
eurjchem-1635	288	7	methane	methane	NOUN
eurjchem-1635	288	8	sulfonamide	sulfonamide	NOUN
eurjchem-1635	288	9	then	then	ADV
eurjchem-1635	288	10	also	also	ADV
eurjchem-1635	288	11	activity	activity	NOUN
eurjchem-1635	288	12	is	be	AUX
eurjchem-1635	288	13	less	less	ADV
eurjchem-1635	288	14	compared	compare	VERB
eurjchem-1635	288	15	to	to	ADP
eurjchem-1635	288	16	aromatic	aromatic	ADJ
eurjchem-1635	288	17	substitutions	substitution	NOUN
eurjchem-1635	288	18	.	.	PUNCT
eurjchem-1635	289	1	these	these	PRON
eurjchem-1635	289	2	are	be	AUX
eurjchem-1635	289	3	results	result	NOUN
eurjchem-1635	289	4	from	from	ADP
eurjchem-1635	289	5	both	both	DET
eurjchem-1635	289	6	series	series	NOUN
eurjchem-1635	289	7	of	of	ADP
eurjchem-1635	289	8	compounds	compound	NOUN
eurjchem-1635	289	9	.	.	PUNCT
eurjchem-1635	290	1	there	there	PRON
eurjchem-1635	290	2	is	be	VERB
eurjchem-1635	290	3	not	not	PART
eurjchem-1635	290	4	much	much	ADJ
eurjchem-1635	290	5	difference	difference	NOUN
eurjchem-1635	290	6	in	in	ADP
eurjchem-1635	290	7	their	their	PRON
eurjchem-1635	290	8	inhibitions	inhibition	NOUN
eurjchem-1635	290	9	in	in	ADP
eurjchem-1635	290	10	all	all	DET
eurjchem-1635	290	11	four	four	NUM
eurjchem-1635	290	12	cancer	cancer	NOUN
eurjchem-1635	290	13	cell	cell	NOUN
eurjchem-1635	290	14	lines	line	NOUN
eurjchem-1635	290	15	.	.	PUNCT
eurjchem-1635	291	1	further	far	ADV
eurjchem-1635	291	2	we	we	PRON
eurjchem-1635	291	3	have	have	AUX
eurjchem-1635	291	4	studied	study	VERB
eurjchem-1635	291	5	the	the	DET
eurjchem-1635	291	6	most	most	ADV
eurjchem-1635	291	7	active	active	ADJ
eurjchem-1635	291	8	compounds	compound	NOUN
eurjchem-1635	291	9	4d	4d	NUM
eurjchem-1635	291	10	,	,	PUNCT
eurjchem-1635	291	11	7c	7c	PROPN
eurjchem-1635	291	12	and	and	CCONJ
eurjchem-1635	291	13	7d	7d	NUM
eurjchem-1635	291	14	on	on	ADP
eurjchem-1635	291	15	human	human	ADJ
eurjchem-1635	291	16	kinases	kinase	NOUN
eurjchem-1635	291	17	.	.	PUNCT
eurjchem-1635	292	1	390	390	NUM
eurjchem-1635	292	2	pawar	pawar	PROPN
eurjchem-1635	292	3	et	et	PROPN
eurjchem-1635	292	4	al	al	PROPN
eurjchem-1635	292	5	.	.	PUNCT
eurjchem-1635	292	6	/	/	SYM
eurjchem-1635	292	7	european	european	PROPN
eurjchem-1635	292	8	journal	journal	PROPN
eurjchem-1635	292	9	of	of	ADP
eurjchem-1635	292	10	chemistry	chemistry	NOUN
eurjchem-1635	292	11	8	8	NUM
eurjchem-1635	292	12	(	(	PUNCT
eurjchem-1635	292	13	4	4	NUM
eurjchem-1635	292	14	)	)	PUNCT
eurjchem-1635	292	15	(	(	PUNCT
eurjchem-1635	292	16	2017	2017	NUM
eurjchem-1635	292	17	)	)	PUNCT
eurjchem-1635	292	18	384‐390	384‐390	NUM
eurjchem-1635	292	19	table	table	NOUN
eurjchem-1635	292	20	4	4	NUM
eurjchem-1635	292	21	inhibitory	inhibitory	ADJ
eurjchem-1635	292	22	activity	activity	NOUN
eurjchem-1635	292	23	of	of	ADP
eurjchem-1635	292	24	compound	compound	NOUN
eurjchem-1635	292	25	4d	4d	NOUN
eurjchem-1635	292	26	,	,	PUNCT
eurjchem-1635	292	27	7c	7c	PROPN
eurjchem-1635	292	28	and	and	CCONJ
eurjchem-1635	292	29	7d	7d	NUM
eurjchem-1635	292	30	against	against	ADP
eurjchem-1635	292	31	panel	panel	NOUN
eurjchem-1635	292	32	of	of	ADP
eurjchem-1635	292	33	eight	eight	NUM
eurjchem-1635	292	34	human	human	ADJ
eurjchem-1635	292	35	kinases	kinase	NOUN
eurjchem-1635	292	36	.	.	PUNCT
eurjchem-1635	293	1	kinase	kinase	PROPN
eurjchem-1635	293	2	%	%	PROPN
eurjchem-1635	293	3	inhibition	inhibition	NOUN
eurjchem-1635	293	4	(	(	PUNCT
eurjchem-1635	293	5	compound	compound	NOUN
eurjchem-1635	293	6	4d	4d	NOUN
eurjchem-1635	293	7	)	)	PUNCT
eurjchem-1635	293	8	%	%	NOUN
eurjchem-1635	293	9	inhibition	inhibition	NOUN
eurjchem-1635	293	10	(	(	PUNCT
eurjchem-1635	293	11	compound	compound	NOUN
eurjchem-1635	293	12	7c	7c	NOUN
eurjchem-1635	293	13	)	)	PUNCT
eurjchem-1635	293	14	%	%	NOUN
eurjchem-1635	293	15	inhibition	inhibition	NOUN
eurjchem-1635	293	16	(	(	PUNCT
eurjchem-1635	293	17	compound	compound	NOUN
eurjchem-1635	293	18	7d	7d	NOUN
eurjchem-1635	293	19	)	)	PUNCT
eurjchem-1635	293	20	aurora‐a	aurora‐a	NOUN
eurjchem-1635	293	21	33	33	NUM
eurjchem-1635	293	22	34	34	NUM
eurjchem-1635	293	23	31	31	NUM
eurjchem-1635	293	24	aurora‐b	aurora‐b	NOUN
eurjchem-1635	293	25	31	31	NUM
eurjchem-1635	293	26	30	30	NUM
eurjchem-1635	293	27	37	37	NUM
eurjchem-1635	293	28	cdk2	cdk2	PROPN
eurjchem-1635	293	29	/	/	SYM
eurjchem-1635	293	30	cyclina	cyclina	PROPN
eurjchem-1635	293	31	28	28	NUM
eurjchem-1635	293	32	37	37	NUM
eurjchem-1635	293	33	43	43	NUM
eurjchem-1635	293	34	cdk2	cdk2	PROPN
eurjchem-1635	293	35	/	/	SYM
eurjchem-1635	293	36	cycline	cycline	PROPN
eurjchem-1635	293	37	17	17	NUM
eurjchem-1635	293	38	12	12	NUM
eurjchem-1635	293	39	11	11	NUM
eurjchem-1635	293	40	cdk5	cdk5	PROPN
eurjchem-1635	293	41	/	/	SYM
eurjchem-1635	293	42	p25	p25	PROPN
eurjchem-1635	293	43	66	66	NUM
eurjchem-1635	293	44	59	59	NUM
eurjchem-1635	293	45	70	70	NUM
eurjchem-1635	293	46	egfr	egfr	NOUN
eurjchem-1635	293	47	4	4	NUM
eurjchem-1635	293	48	21	21	NUM
eurjchem-1635	293	49	15	15	NUM
eurjchem-1635	293	50	mtor	mtor	NOUN
eurjchem-1635	293	51	34	34	NUM
eurjchem-1635	293	52	38	38	NUM
eurjchem-1635	293	53	36	36	NUM
eurjchem-1635	293	54	pdk1	pdk1	NOUN
eurjchem-1635	293	55	13	13	NUM
eurjchem-1635	293	56	21	21	NUM
eurjchem-1635	293	57	9	9	NUM
eurjchem-1635	293	58	the	the	DET
eurjchem-1635	293	59	most	most	ADV
eurjchem-1635	293	60	active	active	ADJ
eurjchem-1635	293	61	compounds	compound	NOUN
eurjchem-1635	293	62	4d	4d	NUM
eurjchem-1635	293	63	,	,	PUNCT
eurjchem-1635	293	64	7c	7c	PROPN
eurjchem-1635	293	65	and	and	CCONJ
eurjchem-1635	293	66	7d	7d	NUM
eurjchem-1635	293	67	were	be	AUX
eurjchem-1635	293	68	tested	test	VERB
eurjchem-1635	293	69	for	for	ADP
eurjchem-1635	293	70	its	its	PRON
eurjchem-1635	293	71	activity	activity	NOUN
eurjchem-1635	293	72	against	against	ADP
eurjchem-1635	293	73	a	a	DET
eurjchem-1635	293	74	panel	panel	NOUN
eurjchem-1635	293	75	of	of	ADP
eurjchem-1635	293	76	eight	eight	NUM
eurjchem-1635	293	77	human	human	ADJ
eurjchem-1635	293	78	kinase	kinase	NOUN
eurjchem-1635	293	79	at	at	ADP
eurjchem-1635	293	80	10	10	NUM
eurjchem-1635	293	81	µm	µm	ADP
eurjchem-1635	293	82	concentrations	concentration	NOUN
eurjchem-1635	293	83	.	.	PUNCT
eurjchem-1635	294	1	the	the	DET
eurjchem-1635	294	2	results	result	NOUN
eurjchem-1635	294	3	are	be	AUX
eurjchem-1635	294	4	summarized	summarize	VERB
eurjchem-1635	294	5	in	in	ADP
eurjchem-1635	294	6	table	table	NOUN
eurjchem-1635	294	7	4	4	NUM
eurjchem-1635	294	8	.	.	PUNCT
eurjchem-1635	295	1	the	the	DET
eurjchem-1635	295	2	compounds	compound	NOUN
eurjchem-1635	295	3	4d	4d	NOUN
eurjchem-1635	295	4	and	and	CCONJ
eurjchem-1635	295	5	7d	7d	NUM
eurjchem-1635	295	6	having	have	VERB
eurjchem-1635	295	7	electron	electron	NOUN
eurjchem-1635	295	8	withdrawing	withdraw	VERB
eurjchem-1635	295	9	group	group	NOUN
eurjchem-1635	295	10	shows	show	VERB
eurjchem-1635	295	11	very	very	ADV
eurjchem-1635	295	12	promising	promising	ADJ
eurjchem-1635	295	13	activity	activity	NOUN
eurjchem-1635	295	14	against	against	ADP
eurjchem-1635	295	15	cdk5	cdk5	PROPN
eurjchem-1635	295	16	/	/	SYM
eurjchem-1635	295	17	p25	p25	PROPN
eurjchem-1635	295	18	kinase	kinase	NOUN
eurjchem-1635	295	19	with	with	ADP
eurjchem-1635	295	20	66	66	NUM
eurjchem-1635	295	21	and	and	CCONJ
eurjchem-1635	295	22	70	70	NUM
eurjchem-1635	295	23	%	%	NOUN
eurjchem-1635	295	24	inhibitions	inhibition	NOUN
eurjchem-1635	295	25	,	,	PUNCT
eurjchem-1635	295	26	respectively	respectively	ADV
eurjchem-1635	295	27	.	.	PUNCT
eurjchem-1635	296	1	compound	compound	NOUN
eurjchem-1635	296	2	7c	7c	PROPN
eurjchem-1635	296	3	also	also	ADV
eurjchem-1635	296	4	shows	show	VERB
eurjchem-1635	296	5	promising	promising	ADJ
eurjchem-1635	296	6	activity	activity	NOUN
eurjchem-1635	296	7	of	of	ADP
eurjchem-1635	296	8	59	59	NUM
eurjchem-1635	296	9	%	%	NOUN
eurjchem-1635	296	10	inhibition	inhibition	NOUN
eurjchem-1635	296	11	.	.	PUNCT
eurjchem-1635	297	1	for	for	ADP
eurjchem-1635	297	2	remaining	remain	VERB
eurjchem-1635	297	3	all	all	DET
eurjchem-1635	297	4	the	the	DET
eurjchem-1635	297	5	kinases	kinase	NOUN
eurjchem-1635	297	6	aurora‐a	aurora‐a	PROPN
eurjchem-1635	297	7	,	,	PUNCT
eurjchem-1635	297	8	aurora‐b	aurora‐b	PROPN
eurjchem-1635	297	9	,	,	PUNCT
eurjchem-1635	297	10	mtor	mtor	PROPN
eurjchem-1635	297	11	and	and	CCONJ
eurjchem-1635	297	12	cdk	cdk	PROPN
eurjchem-1635	297	13	/	/	SYM
eurjchem-1635	297	14	cyclina	cyclina	PROPN
eurjchem-1635	297	15	shows	show	VERB
eurjchem-1635	297	16	moderate	moderate	ADJ
eurjchem-1635	297	17	activity	activity	NOUN
eurjchem-1635	297	18	in	in	ADP
eurjchem-1635	297	19	the	the	DET
eurjchem-1635	297	20	range	range	NOUN
eurjchem-1635	297	21	of	of	ADP
eurjchem-1635	297	22	28	28	NUM
eurjchem-1635	297	23	to	to	PART
eurjchem-1635	297	24	43	43	NUM
eurjchem-1635	297	25	%	%	NOUN
eurjchem-1635	297	26	inhibitions	inhibition	NOUN
eurjchem-1635	297	27	.	.	PUNCT
eurjchem-1635	298	1	for	for	ADP
eurjchem-1635	298	2	remaining	remain	VERB
eurjchem-1635	298	3	kinase	kinase	PROPN
eurjchem-1635	298	4	cdk	cdk	PROPN
eurjchem-1635	298	5	/	/	SYM
eurjchem-1635	298	6	cycline	cycline	PROPN
eurjchem-1635	298	7	,	,	PUNCT
eurjchem-1635	298	8	pdk1	pdk1	NOUN
eurjchem-1635	298	9	and	and	CCONJ
eurjchem-1635	298	10	egfr	egfr	VERB
eurjchem-1635	298	11	the	the	DET
eurjchem-1635	298	12	activity	activity	NOUN
eurjchem-1635	298	13	is	be	AUX
eurjchem-1635	298	14	poor	poor	ADJ
eurjchem-1635	298	15	in	in	ADP
eurjchem-1635	298	16	the	the	DET
eurjchem-1635	298	17	range	range	NOUN
eurjchem-1635	298	18	of	of	ADP
eurjchem-1635	298	19	4	4	NUM
eurjchem-1635	298	20	to	to	PART
eurjchem-1635	298	21	21	21	NUM
eurjchem-1635	298	22	%	%	NOUN
eurjchem-1635	298	23	inhibitions	inhibition	NOUN
eurjchem-1635	298	24	.	.	PUNCT
eurjchem-1635	299	1	from	from	ADP
eurjchem-1635	299	2	all	all	PRON
eurjchem-1635	299	3	above	above	ADP
eurjchem-1635	299	4	ic50	ic50	PROPN
eurjchem-1635	299	5	values	value	NOUN
eurjchem-1635	299	6	and	and	CCONJ
eurjchem-1635	299	7	the	the	DET
eurjchem-1635	299	8	%	%	NOUN
eurjchem-1635	299	9	inhibitions	inhibition	NOUN
eurjchem-1635	299	10	study	study	NOUN
eurjchem-1635	299	11	,	,	PUNCT
eurjchem-1635	299	12	the	the	DET
eurjchem-1635	299	13	sar	sar	NOUN
eurjchem-1635	299	14	can	can	AUX
eurjchem-1635	299	15	be	be	AUX
eurjchem-1635	299	16	explained	explain	VERB
eurjchem-1635	299	17	on	on	ADP
eurjchem-1635	299	18	the	the	DET
eurjchem-1635	299	19	basis	basis	NOUN
eurjchem-1635	299	20	of	of	ADP
eurjchem-1635	299	21	substitutions	substitution	NOUN
eurjchem-1635	299	22	on	on	ADP
eurjchem-1635	299	23	the	the	DET
eurjchem-1635	299	24	r1	r1	PROPN
eurjchem-1635	299	25	position	position	NOUN
eurjchem-1635	299	26	with	with	ADP
eurjchem-1635	299	27	aromatic	aromatic	ADJ
eurjchem-1635	299	28	or	or	CCONJ
eurjchem-1635	299	29	aliphatic	aliphatic	ADJ
eurjchem-1635	299	30	substitution	substitution	NOUN
eurjchem-1635	299	31	.	.	PUNCT
eurjchem-1635	300	1	the	the	DET
eurjchem-1635	300	2	com‐	com‐	ADJ
eurjchem-1635	300	3	pounds	pound	NOUN
eurjchem-1635	300	4	containing	contain	VERB
eurjchem-1635	300	5	electron	electron	NOUN
eurjchem-1635	300	6	withdrawing	withdraw	VERB
eurjchem-1635	300	7	groups	group	NOUN
eurjchem-1635	300	8	on	on	ADP
eurjchem-1635	300	9	r1	r1	NOUN
eurjchem-1635	300	10	phenyl	phenyl	NOUN
eurjchem-1635	300	11	ring	ring	NOUN
eurjchem-1635	300	12	show	show	VERB
eurjchem-1635	300	13	good	good	ADJ
eurjchem-1635	300	14	to	to	ADP
eurjchem-1635	300	15	moderate	moderate	ADJ
eurjchem-1635	300	16	activity	activity	NOUN
eurjchem-1635	300	17	(	(	PUNCT
eurjchem-1635	300	18	compound	compound	NOUN
eurjchem-1635	300	19	4c	4c	NOUN
eurjchem-1635	300	20	,	,	PUNCT
eurjchem-1635	300	21	4d	4d	NUM
eurjchem-1635	300	22	,	,	PUNCT
eurjchem-1635	300	23	7c	7c	PROPN
eurjchem-1635	300	24	and	and	CCONJ
eurjchem-1635	300	25	7d	7d	NUM
eurjchem-1635	300	26	)	)	PUNCT
eurjchem-1635	300	27	when	when	SCONJ
eurjchem-1635	300	28	compared	compare	VERB
eurjchem-1635	300	29	with	with	ADP
eurjchem-1635	300	30	the	the	DET
eurjchem-1635	300	31	other	other	ADJ
eurjchem-1635	300	32	simple	simple	ADJ
eurjchem-1635	300	33	substitution	substitution	NOUN
eurjchem-1635	300	34	on	on	ADP
eurjchem-1635	300	35	r1	r1	PROPN
eurjchem-1635	300	36	phenyl	phenyl	NOUN
eurjchem-1635	300	37	ring	ring	NOUN
eurjchem-1635	300	38	.	.	PUNCT
eurjchem-1635	301	1	very	very	ADV
eurjchem-1635	301	2	low	low	ADJ
eurjchem-1635	301	3	activity	activity	NOUN
eurjchem-1635	301	4	is	be	AUX
eurjchem-1635	301	5	observed	observe	VERB
eurjchem-1635	301	6	with	with	ADP
eurjchem-1635	301	7	the	the	DET
eurjchem-1635	301	8	substitution	substitution	NOUN
eurjchem-1635	301	9	of	of	ADP
eurjchem-1635	301	10	electron	electron	NOUN
eurjchem-1635	301	11	donating	donate	VERB
eurjchem-1635	301	12	methyl	methyl	NOUN
eurjchem-1635	301	13	group	group	NOUN
eurjchem-1635	301	14	on	on	ADP
eurjchem-1635	301	15	the	the	DET
eurjchem-1635	301	16	phenyl	phenyl	NOUN
eurjchem-1635	301	17	ring	ring	NOUN
eurjchem-1635	301	18	.	.	PUNCT
eurjchem-1635	302	1	4	4	X
eurjchem-1635	302	2	.	.	X
eurjchem-1635	302	3	conclusion	conclusion	NOUN
eurjchem-1635	302	4	this	this	PRON
eurjchem-1635	302	5	reported	report	VERB
eurjchem-1635	302	6	work	work	NOUN
eurjchem-1635	302	7	deals	deal	NOUN
eurjchem-1635	302	8	with	with	ADP
eurjchem-1635	302	9	the	the	DET
eurjchem-1635	302	10	non‐asymmetric	non‐asymmetric	ADJ
eurjchem-1635	302	11	synthesis	synthesis	NOUN
eurjchem-1635	302	12	of	of	ADP
eurjchem-1635	302	13	benzoxazine	benzoxazine	NOUN
eurjchem-1635	302	14	derivatives	derivative	NOUN
eurjchem-1635	302	15	and	and	CCONJ
eurjchem-1635	302	16	their	their	PRON
eurjchem-1635	302	17	evaluation	evaluation	NOUN
eurjchem-1635	302	18	as	as	ADP
eurjchem-1635	302	19	antiproliferative	antiproliferative	ADJ
eurjchem-1635	302	20	agents	agent	NOUN
eurjchem-1635	302	21	against	against	ADP
eurjchem-1635	302	22	different	different	ADJ
eurjchem-1635	302	23	cancer	cancer	NOUN
eurjchem-1635	302	24	cell	cell	NOUN
eurjchem-1635	302	25	lines	line	NOUN
eurjchem-1635	302	26	and	and	CCONJ
eurjchem-1635	302	27	in	in	ADP
eurjchem-1635	302	28	the	the	DET
eurjchem-1635	302	29	growth	growth	NOUN
eurjchem-1635	302	30	of	of	ADP
eurjchem-1635	302	31	eight	eight	NUM
eurjchem-1635	302	32	human	human	ADJ
eurjchem-1635	302	33	kinases	kinase	NOUN
eurjchem-1635	302	34	.	.	PUNCT
eurjchem-1635	303	1	the	the	DET
eurjchem-1635	303	2	obtained	obtain	VERB
eurjchem-1635	303	3	yields	yield	NOUN
eurjchem-1635	303	4	were	be	AUX
eurjchem-1635	303	5	good	good	ADJ
eurjchem-1635	303	6	to	to	PART
eurjchem-1635	303	7	excellent	excellent	VERB
eurjchem-1635	303	8	with	with	ADP
eurjchem-1635	303	9	high	high	ADJ
eurjchem-1635	303	10	purity	purity	NOUN
eurjchem-1635	303	11	.	.	PUNCT
eurjchem-1635	304	1	the	the	DET
eurjchem-1635	304	2	compounds	compound	NOUN
eurjchem-1635	304	3	were	be	AUX
eurjchem-1635	304	4	synthesized	synthesize	VERB
eurjchem-1635	304	5	on	on	ADP
eurjchem-1635	304	6	gram	gram	NOUN
eurjchem-1635	304	7	scale	scale	NOUN
eurjchem-1635	304	8	by	by	ADP
eurjchem-1635	304	9	using	use	VERB
eurjchem-1635	304	10	series	series	NOUN
eurjchem-1635	304	11	of	of	ADP
eurjchem-1635	304	12	reactions	reaction	NOUN
eurjchem-1635	304	13	having	have	VERB
eurjchem-1635	304	14	reduction	reduction	NOUN
eurjchem-1635	304	15	and	and	CCONJ
eurjchem-1635	304	16	coupling	coupling	NOUN
eurjchem-1635	304	17	reactions	reaction	NOUN
eurjchem-1635	304	18	.	.	PUNCT
eurjchem-1635	305	1	we	we	PRON
eurjchem-1635	305	2	have	have	AUX
eurjchem-1635	305	3	optimized	optimize	VERB
eurjchem-1635	305	4	all	all	DET
eurjchem-1635	305	5	the	the	DET
eurjchem-1635	305	6	reaction	reaction	NOUN
eurjchem-1635	305	7	steps	step	NOUN
eurjchem-1635	305	8	for	for	ADP
eurjchem-1635	305	9	getting	get	VERB
eurjchem-1635	305	10	good	good	ADJ
eurjchem-1635	305	11	yields	yield	NOUN
eurjchem-1635	305	12	.	.	PUNCT
eurjchem-1635	306	1	the	the	DET
eurjchem-1635	306	2	compounds	compound	NOUN
eurjchem-1635	306	3	4c	4c	NOUN
eurjchem-1635	306	4	,	,	PUNCT
eurjchem-1635	306	5	4d	4d	NUM
eurjchem-1635	306	6	,	,	PUNCT
eurjchem-1635	306	7	7c	7c	PROPN
eurjchem-1635	306	8	and	and	CCONJ
eurjchem-1635	306	9	7d	7d	NUM
eurjchem-1635	306	10	were	be	AUX
eurjchem-1635	306	11	found	find	VERB
eurjchem-1635	306	12	to	to	PART
eurjchem-1635	306	13	be	be	AUX
eurjchem-1635	306	14	most	most	ADV
eurjchem-1635	306	15	active	active	ADJ
eurjchem-1635	306	16	on	on	ADP
eurjchem-1635	306	17	the	the	DET
eurjchem-1635	306	18	treated	treat	VERB
eurjchem-1635	306	19	cell	cell	NOUN
eurjchem-1635	306	20	lines	line	NOUN
eurjchem-1635	306	21	,	,	PUNCT
eurjchem-1635	306	22	and	and	CCONJ
eurjchem-1635	306	23	compound	compound	NOUN
eurjchem-1635	306	24	4d	4d	NUM
eurjchem-1635	306	25	,	,	PUNCT
eurjchem-1635	306	26	7c	7c	PROPN
eurjchem-1635	306	27	and	and	CCONJ
eurjchem-1635	306	28	7d	7d	NUM
eurjchem-1635	306	29	shows	show	NOUN
eurjchem-1635	306	30	promising	promise	VERB
eurjchem-1635	306	31	activity	activity	NOUN
eurjchem-1635	306	32	against	against	ADP
eurjchem-1635	306	33	cdk5	cdk5	PROPN
eurjchem-1635	306	34	/	/	SYM
eurjchem-1635	306	35	p25	p25	PROPN
eurjchem-1635	306	36	kinase	kinase	NOUN
eurjchem-1635	306	37	inhibitors	inhibitor	NOUN
eurjchem-1635	306	38	.	.	PUNCT
eurjchem-1635	307	1	acknowledgements	acknowledgement	NOUN
eurjchem-1635	307	2	the	the	DET
eurjchem-1635	307	3	authors	author	NOUN
eurjchem-1635	307	4	are	be	AUX
eurjchem-1635	307	5	thankful	thankful	ADJ
eurjchem-1635	307	6	to	to	ADP
eurjchem-1635	307	7	the	the	DET
eurjchem-1635	307	8	head	head	NOUN
eurjchem-1635	307	9	,	,	PUNCT
eurjchem-1635	307	10	department	department	NOUN
eurjchem-1635	307	11	of	of	ADP
eurjchem-1635	307	12	chemical	chemical	PROPN
eurjchem-1635	307	13	technology	technology	PROPN
eurjchem-1635	307	14	,	,	PUNCT
eurjchem-1635	307	15	dr	dr	PROPN
eurjchem-1635	307	16	.	.	PROPN
eurjchem-1635	307	17	babasaheb	babasaheb	PROPN
eurjchem-1635	307	18	ambedkar	ambedkar	PROPN
eurjchem-1635	307	19	marathwada	marathwada	PROPN
eurjchem-1635	307	20	university	university	PROPN
eurjchem-1635	307	21	,	,	PUNCT
eurjchem-1635	307	22	aurangabad	aurangabad	PROPN
eurjchem-1635	307	23	431004	431004	NUM
eurjchem-1635	307	24	,	,	PUNCT
eurjchem-1635	307	25	ms	ms	PROPN
eurjchem-1635	307	26	,	,	PUNCT
eurjchem-1635	307	27	india	india	PROPN
eurjchem-1635	307	28	for	for	ADP
eurjchem-1635	307	29	providing	provide	VERB
eurjchem-1635	307	30	the	the	DET
eurjchem-1635	307	31	laboratory	laboratory	NOUN
eurjchem-1635	307	32	facility	facility	NOUN
eurjchem-1635	307	33	.	.	PUNCT
eurjchem-1635	308	1	references	reference	NOUN
eurjchem-1635	308	2	[	[	X
eurjchem-1635	308	3	1	1	NUM
eurjchem-1635	308	4	]	]	PUNCT
eurjchem-1635	308	5	.	.	PUNCT
eurjchem-1635	309	1	alafeefy	alafeefy	PROPN
eurjchem-1635	309	2	,	,	PUNCT
eurjchem-1635	309	3	a.	a.	NOUN
eurjchem-1635	309	4	m.	m.	NOUN
eurjchem-1635	309	5	;	;	PUNCT
eurjchem-1635	309	6	ashour	ashour	PROPN
eurjchem-1635	309	7	,	,	PUNCT
eurjchem-1635	309	8	a.	a.	PROPN
eurjchem-1635	309	9	e.	e.	PROPN
eurjchem-1635	309	10	;	;	PUNCT
eurjchem-1635	309	11	prasad	prasad	PROPN
eurjchem-1635	309	12	,	,	PUNCT
eurjchem-1635	309	13	o.	o.	PROPN
eurjchem-1635	309	14	;	;	PUNCT
eurjchem-1635	309	15	sinha	sinha	PROPN
eurjchem-1635	309	16	,	,	PUNCT
eurjchem-1635	309	17	l.	l.	PROPN
eurjchem-1635	309	18	;	;	PUNCT
eurjchem-1635	309	19	pathak	pathak	PROPN
eurjchem-1635	309	20	,	,	PUNCT
eurjchem-1635	309	21	s.	s.	PROPN
eurjchem-1635	309	22	;	;	PUNCT
eurjchem-1635	309	23	alasmari	alasmari	PROPN
eurjchem-1635	309	24	,	,	PUNCT
eurjchem-1635	309	25	f.	f.	PROPN
eurjchem-1635	309	26	a.	a.	PROPN
eurjchem-1635	309	27	;	;	PUNCT
eurjchem-1635	309	28	rishi	rishi	PROPN
eurjchem-1635	309	29	,	,	PUNCT
eurjchem-1635	309	30	a.	a.	PROPN
eurjchem-1635	309	31	k.	k.	PROPN
eurjchem-1635	309	32	;	;	PUNCT
eurjchem-1635	309	33	abdel‐aziz	abdel‐aziz	PROPN
eurjchem-1635	309	34	,	,	PUNCT
eurjchem-1635	309	35	h.	h.	PROPN
eurjchem-1635	309	36	a.	a.	PROPN
eurjchem-1635	309	37	eur	eur	PROPN
eurjchem-1635	309	38	.	.	PUNCT
eurjchem-1635	310	1	j.	j.	PROPN
eurjchem-1635	310	2	med	med	PROPN
eurjchem-1635	310	3	.	.	PROPN
eurjchem-1635	310	4	chem	chem	PROPN
eurjchem-1635	310	5	.	.	PUNCT
eurjchem-1635	311	1	2015	2015	NUM
eurjchem-1635	311	2	,	,	PUNCT
eurjchem-1635	311	3	92	92	NUM
eurjchem-1635	311	4	,	,	PUNCT
eurjchem-1635	311	5	191‐201	191‐201	NUM
eurjchem-1635	311	6	.	.	PUNCT
eurjchem-1635	312	1	[	[	X
eurjchem-1635	312	2	2	2	NUM
eurjchem-1635	312	3	]	]	PUNCT
eurjchem-1635	312	4	.	.	PUNCT
eurjchem-1635	313	1	alberg	alberg	PROPN
eurjchem-1635	313	2	,	,	PUNCT
eurjchem-1635	313	3	a.	a.	PROPN
eurjchem-1635	313	4	j.	j.	PROPN
eurjchem-1635	313	5	;	;	PUNCT
eurjchem-1635	313	6	brock	brock	PROPN
eurjchem-1635	313	7	,	,	PUNCT
eurjchem-1635	313	8	m.	m.	NOUN
eurjchem-1635	313	9	v.	v.	PROPN
eurjchem-1635	313	10	;	;	PUNCT
eurjchem-1635	313	11	samet	samet	PROPN
eurjchem-1635	313	12	,	,	PUNCT
eurjchem-1635	313	13	j.	j.	PROPN
eurjchem-1635	313	14	m.	m.	PROPN
eurjchem-1635	313	15	j.	j.	PROPN
eurjchem-1635	313	16	clin	clin	PROPN
eurjchem-1635	313	17	.	.	PUNCT
eurjchem-1635	314	1	oncol	oncol	ADJ
eurjchem-1635	314	2	.	.	PUNCT
eurjchem-1635	315	1	2005	2005	NUM
eurjchem-1635	315	2	,	,	PUNCT
eurjchem-1635	315	3	23	23	NUM
eurjchem-1635	315	4	,	,	PUNCT
eurjchem-1635	315	5	3175‐	3175‐	NUM
eurjchem-1635	315	6	3185	3185	NUM
eurjchem-1635	315	7	.	.	PUNCT
eurjchem-1635	316	1	[	[	X
eurjchem-1635	316	2	3	3	NUM
eurjchem-1635	316	3	]	]	PUNCT
eurjchem-1635	316	4	.	.	PUNCT
eurjchem-1635	317	1	zhou	zhou	PROPN
eurjchem-1635	317	2	,	,	PUNCT
eurjchem-1635	317	3	x.	x.	PROPN
eurjchem-1635	317	4	w.	w.	PROPN
eurjchem-1635	317	5	;	;	PUNCT
eurjchem-1635	317	6	ma	ma	PROPN
eurjchem-1635	317	7	,	,	PUNCT
eurjchem-1635	317	8	h.	h.	PROPN
eurjchem-1635	317	9	l.	l.	PROPN
eurjchem-1635	317	10	;	;	PUNCT
eurjchem-1635	317	11	zhang	zhang	PROPN
eurjchem-1635	317	12	,	,	PUNCT
eurjchem-1635	317	13	x.	x.	PROPN
eurjchem-1635	317	14	;	;	PUNCT
eurjchem-1635	317	15	jing	jing	PROPN
eurjchem-1635	317	16	,	,	PUNCT
eurjchem-1635	317	17	s.	s.	PROPN
eurjchem-1635	317	18	y.	y.	PROPN
eurjchem-1635	317	19	;	;	PUNCT
eurjchem-1635	317	20	miao	miao	PROPN
eurjchem-1635	317	21	,	,	PUNCT
eurjchem-1635	317	22	j.	j.	PROPN
eurjchem-1635	317	23	y.	y.	PROPN
eurjchem-1635	317	24	;	;	PUNCT
eurjchem-1635	317	25	zhao	zhao	PROPN
eurjchem-1635	317	26	,	,	PUNCT
eurjchem-1635	317	27	b.	b.	PROPN
eurjchem-1635	317	28	x.	x.	PROPN
eurjchem-1635	317	29	eur	eur	PROPN
eurjchem-1635	317	30	.	.	PUNCT
eurjchem-1635	318	1	j.	j.	PROPN
eurjchem-1635	318	2	med	med	PROPN
eurjchem-1635	318	3	.	.	PROPN
eurjchem-1635	318	4	chem	chem	PROPN
eurjchem-1635	318	5	.	.	PUNCT
eurjchem-1635	319	1	2014	2014	NUM
eurjchem-1635	319	2	,	,	PUNCT
eurjchem-1635	319	3	79	79	NUM
eurjchem-1635	319	4	,	,	PUNCT
eurjchem-1635	319	5	95‐101	95‐101	NUM
eurjchem-1635	319	6	.	.	PUNCT
eurjchem-1635	320	1	[	[	X
eurjchem-1635	320	2	4	4	NUM
eurjchem-1635	320	3	]	]	PUNCT
eurjchem-1635	320	4	.	.	PUNCT
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eurjchem-1635	321	2	,	,	PUNCT
eurjchem-1635	321	3	s.	s.	PROPN
eurjchem-1635	321	4	;	;	PUNCT
eurjchem-1635	321	5	su	su	PROPN
eurjchem-1635	321	6	,	,	PUNCT
eurjchem-1635	321	7	h.	h.	PROPN
eurjchem-1635	321	8	;	;	PUNCT
eurjchem-1635	321	9	zhao	zhao	PROPN
eurjchem-1635	321	10	,	,	PUNCT
eurjchem-1635	321	11	b.	b.	PROPN
eurjchem-1635	321	12	x.	x.	PROPN
eurjchem-1635	321	13	;	;	PUNCT
eurjchem-1635	321	14	liu	liu	PROPN
eurjchem-1635	321	15	,	,	PUNCT
eurjchem-1635	321	16	w.	w.	PROPN
eurjchem-1635	321	17	y.	y.	PROPN
eurjchem-1635	321	18	;	;	PUNCT
eurjchem-1635	321	19	zheng	zheng	PROPN
eurjchem-1635	321	20	,	,	PUNCT
eurjchem-1635	321	21	l.w	l.w	PROPN
eurjchem-1635	321	22	.	.	PROPN
eurjchem-1635	321	23	;	;	PUNCT
eurjchem-1635	321	24	miao	miao	PROPN
eurjchem-1635	321	25	,	,	PUNCT
eurjchem-1635	321	26	j.	j.	PROPN
eurjchem-1635	321	27	y.	y.	PROPN
eurjchem-1635	321	28	bioorg	bioorg	PROPN
eurjchem-1635	321	29	.	.	PUNCT
eurjchem-1635	322	1	med	med	PROPN
eurjchem-1635	322	2	.	.	PUNCT
eurjchem-1635	322	3	chem	chem	PROPN
eurjchem-1635	322	4	.	.	PUNCT
eurjchem-1635	323	1	2009	2009	NUM
eurjchem-1635	323	2	,	,	PUNCT
eurjchem-1635	323	3	17	17	NUM
eurjchem-1635	323	4	,	,	PUNCT
eurjchem-1635	323	5	7085‐7092	7085‐7092	NUM
eurjchem-1635	323	6	.	.	PUNCT
eurjchem-1635	324	1	[	[	X
eurjchem-1635	324	2	5	5	NUM
eurjchem-1635	324	3	]	]	PUNCT
eurjchem-1635	324	4	.	.	PUNCT
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eurjchem-1635	325	4	;	;	PUNCT
eurjchem-1635	325	5	prouty	prouty	NOUN
eurjchem-1635	325	6	,	,	PUNCT
eurjchem-1635	325	7	c.	c.	PROPN
eurjchem-1635	325	8	p.	p.	PROPN
eurjchem-1635	325	9	;	;	PUNCT
eurjchem-1635	325	10	pelton	pelton	PROPN
eurjchem-1635	325	11	,	,	PUNCT
eurjchem-1635	325	12	p.	p.	PROPN
eurjchem-1635	325	13	d.	d.	PROPN
eurjchem-1635	325	14	;	;	PUNCT
eurjchem-1635	325	15	yong	yong	PROPN
eurjchem-1635	325	16	,	,	PUNCT
eurjchem-1635	325	17	m.	m.	NOUN
eurjchem-1635	325	18	;	;	PUNCT
eurjchem-1635	325	19	demarest	demarest	PROPN
eurjchem-1635	325	20	,	,	PUNCT
eurjchem-1635	325	21	k.	k.	PROPN
eurjchem-1635	325	22	t.	t.	PROPN
eurjchem-1635	325	23	;	;	PUNCT
eurjchem-1635	325	24	murray	murray	PROPN
eurjchem-1635	325	25	,	,	PUNCT
eurjchem-1635	325	26	w.	w.	PROPN
eurjchem-1635	325	27	v.	v.	PROPN
eurjchem-1635	325	28	;	;	PUNCT
eurjchem-1635	325	29	kuo	kuo	PROPN
eurjchem-1635	325	30	,	,	PUNCT
eurjchem-1635	325	31	g.	g.	PROPN
eurjchem-1635	325	32	h.	h.	PROPN
eurjchem-1635	325	33	bioorg	bioorg	PROPN
eurjchem-1635	325	34	.	.	PUNCT
eurjchem-1635	326	1	med	med	PROPN
eurjchem-1635	326	2	.	.	PROPN
eurjchem-1635	326	3	chem	chem	PROPN
eurjchem-1635	326	4	.	.	PUNCT
eurjchem-1635	327	1	2010	2010	NUM
eurjchem-1635	327	2	,	,	PUNCT
eurjchem-1635	327	3	20	20	NUM
eurjchem-1635	327	4	,	,	PUNCT
eurjchem-1635	327	5	1432‐1435	1432‐1435	NUM
eurjchem-1635	327	6	.	.	PUNCT
eurjchem-1635	328	1	[	[	X
eurjchem-1635	328	2	6	6	NUM
eurjchem-1635	328	3	]	]	PUNCT
eurjchem-1635	328	4	.	.	PUNCT
eurjchem-1635	329	1	matralis	matralis	PROPN
eurjchem-1635	329	2	,	,	PUNCT
eurjchem-1635	329	3	a.	a.	NOUN
eurjchem-1635	329	4	n.	n.	NOUN
eurjchem-1635	329	5	;	;	PUNCT
eurjchem-1635	329	6	katselou	katselou	PROPN
eurjchem-1635	329	7	,	,	PUNCT
eurjchem-1635	329	8	m.	m.	NOUN
eurjchem-1635	329	9	g.	g.	PROPN
eurjchem-1635	329	10	;	;	PUNCT
eurjchem-1635	329	11	nikitakis	nikitakis	PROPN
eurjchem-1635	329	12	,	,	PUNCT
eurjchem-1635	329	13	a.	a.	NOUN
eurjchem-1635	329	14	;	;	PUNCT
eurjchem-1635	329	15	kourounakis	kourounaki	NOUN
eurjchem-1635	329	16	,	,	PUNCT
eurjchem-1635	330	1	a.	a.	NOUN
eurjchem-1635	330	2	p.	p.	PROPN
eurjchem-1635	330	3	j.	j.	PROPN
eurjchem-1635	330	4	med	med	PROPN
eurjchem-1635	330	5	.	.	PUNCT
eurjchem-1635	330	6	chem	chem	PROPN
eurjchem-1635	330	7	.	.	PUNCT
eurjchem-1635	331	1	2011	2011	NUM
eurjchem-1635	331	2	,	,	PUNCT
eurjchem-1635	331	3	54	54	NUM
eurjchem-1635	331	4	,	,	PUNCT
eurjchem-1635	331	5	5583‐5591	5583‐5591	NUM
eurjchem-1635	331	6	.	.	PUNCT
eurjchem-1635	332	1	[	[	X
eurjchem-1635	332	2	7	7	NUM
eurjchem-1635	332	3	]	]	PUNCT
eurjchem-1635	332	4	.	.	PUNCT
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eurjchem-1635	333	2	,	,	PUNCT
eurjchem-1635	333	3	t.	t.	PROPN
eurjchem-1635	333	4	;	;	PUNCT
eurjchem-1635	333	5	matsunaga	matsunaga	NOUN
eurjchem-1635	333	6	,	,	PUNCT
eurjchem-1635	333	7	n.	n.	NOUN
eurjchem-1635	333	8	;	;	PUNCT
eurjchem-1635	333	9	ora	ora	PROPN
eurjchem-1635	333	10	,	,	PUNCT
eurjchem-1635	333	11	t.	t.	NOUN
eurjchem-1635	333	12	;	;	PUNCT
eurjchem-1635	333	13	ohyabu	ohyabu	ADV
eurjchem-1635	333	14	,	,	PUNCT
eurjchem-1635	333	15	n.	n.	NOUN
eurjchem-1635	333	16	;	;	PUNCT
eurjchem-1635	333	17	nishigaki	nishigaki	NOUN
eurjchem-1635	333	18	,	,	PUNCT
eurjchem-1635	333	19	n.	n.	NOUN
eurjchem-1635	333	20	;	;	PUNCT
eurjchem-1635	333	21	imura	imura	NOUN
eurjchem-1635	333	22	,	,	PUNCT
eurjchem-1635	333	23	y.	y.	PROPN
eurjchem-1635	333	24	;	;	PUNCT
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eurjchem-1635	333	26	,	,	PUNCT
eurjchem-1635	333	27	y.	y.	PROPN
eurjchem-1635	333	28	;	;	PUNCT
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eurjchem-1635	333	30	,	,	PUNCT
eurjchem-1635	333	31	h.	h.	PROPN
eurjchem-1635	333	32	;	;	PUNCT
eurjchem-1635	333	33	motoyaji	motoyaji	PROPN
eurjchem-1635	333	34	,	,	PUNCT
eurjchem-1635	333	35	t.	t.	PROPN
eurjchem-1635	333	36	;	;	PUNCT
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eurjchem-1635	333	38	,	,	PUNCT
eurjchem-1635	333	39	t.	t.	PROPN
eurjchem-1635	333	40	;	;	PUNCT
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eurjchem-1635	333	42	,	,	PUNCT
eurjchem-1635	333	43	n.	n.	NOUN
eurjchem-1635	333	44	;	;	PUNCT
eurjchem-1635	333	45	sogabe	sogabe	PROPN
eurjchem-1635	333	46	,	,	PUNCT
eurjchem-1635	333	47	s.	s.	PROPN
eurjchem-1635	333	48	;	;	PUNCT
eurjchem-1635	333	49	ono	ono	PROPN
eurjchem-1635	333	50	,	,	PUNCT
eurjchem-1635	333	51	m.	m.	NOUN
eurjchem-1635	333	52	;	;	PUNCT
eurjchem-1635	333	53	siedem	siedem	PROPN
eurjchem-1635	333	54	,	,	PUNCT
eurjchem-1635	333	55	c.s	c.s	PROPN
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eurjchem-1635	333	57	;	;	PUNCT
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eurjchem-1635	333	60	t.	t.	PROPN
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eurjchem-1635	333	62	;	;	PUNCT
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eurjchem-1635	333	65	c.	c.	PROPN
eurjchem-1635	333	66	;	;	PUNCT
eurjchem-1635	333	67	de	de	X
eurjchem-1635	333	68	meese	meese	PROPN
eurjchem-1635	333	69	,	,	PUNCT
eurjchem-1635	333	70	l.	l.	PROPN
eurjchem-1635	333	71	a.	a.	PROPN
eurjchem-1635	333	72	;	;	PUNCT
eurjchem-1635	333	73	boyd	boyd	PROPN
eurjchem-1635	333	74	,	,	PUNCT
eurjchem-1635	333	75	s.	s.	PROPN
eurjchem-1635	333	76	a.	a.	PROPN
eurjchem-1635	333	77	;	;	PUNCT
eurjchem-1635	333	78	fukumoto	fukumoto	PROPN
eurjchem-1635	333	79	,	,	PUNCT
eurjchem-1635	333	80	s.	s.	PROPN
eurjchem-1635	333	81	j.	j.	PROPN
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eurjchem-1635	333	83	.	.	PROPN
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eurjchem-1635	333	85	.	.	PUNCT
eurjchem-1635	334	1	2011	2011	NUM
eurjchem-1635	334	2	,	,	PUNCT
eurjchem-1635	334	3	54	54	NUM
eurjchem-1635	334	4	,	,	PUNCT
eurjchem-1635	334	5	8616‐8631	8616‐8631	NUM
eurjchem-1635	334	6	.	.	PUNCT
eurjchem-1635	335	1	[	[	X
eurjchem-1635	335	2	8	8	NUM
eurjchem-1635	335	3	]	]	PUNCT
eurjchem-1635	335	4	.	.	PUNCT
eurjchem-1635	336	1	filippou	filippou	NUM
eurjchem-1635	336	2	,	,	PUNCT
eurjchem-1635	336	3	p.	p.	NOUN
eurjchem-1635	336	4	s.	s.	PROPN
eurjchem-1635	336	5	;	;	PUNCT
eurjchem-1635	337	1	koini	koini	PROPN
eurjchem-1635	337	2	,	,	PUNCT
eurjchem-1635	337	3	e.	e.	PROPN
eurjchem-1635	337	4	n.	n.	PROPN
eurjchem-1635	337	5	;	;	PUNCT
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eurjchem-1635	337	7	,	,	PUNCT
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eurjchem-1635	337	9	;	;	PUNCT
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eurjchem-1635	337	13	;	;	PUNCT
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eurjchem-1635	337	17	a.	a.	PROPN
eurjchem-1635	337	18	;	;	PUNCT
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eurjchem-1635	337	20	,	,	PUNCT
eurjchem-1635	337	21	d.	d.	PROPN
eurjchem-1635	337	22	a.	a.	PROPN
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eurjchem-1635	337	24	.	.	PUNCT
eurjchem-1635	338	1	med	med	PROPN
eurjchem-1635	338	2	.	.	PROPN
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eurjchem-1635	338	4	.	.	PUNCT
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eurjchem-1635	339	2	.	.	PUNCT
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eurjchem-1635	340	2	,	,	PUNCT
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eurjchem-1635	340	4	,	,	PUNCT
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eurjchem-1635	340	6	.	.	PUNCT
eurjchem-1635	341	1	[	[	X
eurjchem-1635	341	2	9	9	NUM
eurjchem-1635	341	3	]	]	PUNCT
eurjchem-1635	341	4	.	.	PUNCT
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eurjchem-1635	342	2	,	,	PUNCT
eurjchem-1635	342	3	b.	b.	PROPN
eurjchem-1635	342	4	;	;	PUNCT
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eurjchem-1635	342	6	,	,	PUNCT
eurjchem-1635	342	7	j.	j.	PROPN
eurjchem-1635	342	8	;	;	PUNCT
eurjchem-1635	342	9	eyermann	eyermann	PROPN
eurjchem-1635	342	10	,	,	PUNCT
eurjchem-1635	342	11	c.	c.	PROPN
eurjchem-1635	342	12	j.	j.	PROPN
eurjchem-1635	342	13	;	;	PUNCT
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eurjchem-1635	342	15	,	,	PUNCT
eurjchem-1635	342	16	f.	f.	PROPN
eurjchem-1635	342	17	;	;	PUNCT
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eurjchem-1635	342	19	,	,	PUNCT
eurjchem-1635	342	20	s.	s.	PROPN
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eurjchem-1635	342	22	.	.	PUNCT
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eurjchem-1635	344	2	.	.	PUNCT
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eurjchem-1635	345	2	,	,	PUNCT
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eurjchem-1635	345	4	,	,	PUNCT
eurjchem-1635	345	5	5432‐5435	5432‐5435	NUM
eurjchem-1635	345	6	.	.	PUNCT
eurjchem-1635	346	1	[	[	X
eurjchem-1635	346	2	10	10	NUM
eurjchem-1635	346	3	]	]	PUNCT
eurjchem-1635	346	4	.	.	PUNCT
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eurjchem-1635	346	9	;	;	PUNCT
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eurjchem-1635	346	14	;	;	PUNCT
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eurjchem-1635	346	17	s.	s.	PROPN
eurjchem-1635	346	18	p.	p.	PROPN
eurjchem-1635	346	19	;	;	PUNCT
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eurjchem-1635	347	2	,	,	PUNCT
eurjchem-1635	347	3	m.	m.	NOUN
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eurjchem-1635	347	5	;	;	PUNCT
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eurjchem-1635	347	7	,	,	PUNCT
eurjchem-1635	347	8	s.	s.	PROPN
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eurjchem-1635	347	10	;	;	PUNCT
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eurjchem-1635	347	13	v.	v.	ADP
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eurjchem-1635	347	15	;	;	PUNCT
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eurjchem-1635	347	18	r.	r.	PROPN
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eurjchem-1635	347	20	;	;	PUNCT
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eurjchem-1635	347	22	,	,	PUNCT
eurjchem-1635	347	23	r.	r.	PROPN
eurjchem-1635	347	24	;	;	PUNCT
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eurjchem-1635	347	29	;	;	PUNCT
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eurjchem-1635	347	32	s.	s.	PROPN
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eurjchem-1635	347	34	;	;	PUNCT
eurjchem-1635	347	35	kunte	kunte	PROPN
eurjchem-1635	347	36	,	,	PUNCT
eurjchem-1635	347	37	s.	s.	PROPN
eurjchem-1635	347	38	s.	s.	PROPN
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eurjchem-1635	347	40	.	.	PUNCT
eurjchem-1635	348	1	med	med	PROPN
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eurjchem-1635	348	4	.	.	PUNCT
eurjchem-1635	349	1	lett	lett	PROPN
eurjchem-1635	349	2	.	.	PUNCT
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eurjchem-1635	350	2	,	,	PUNCT
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eurjchem-1635	350	4	,	,	PUNCT
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eurjchem-1635	350	6	.	.	PUNCT
eurjchem-1635	351	1	[	[	X
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eurjchem-1635	351	3	]	]	PUNCT
eurjchem-1635	351	4	.	.	PUNCT
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eurjchem-1635	352	2	,	,	PUNCT
eurjchem-1635	352	3	r.	r.	PROPN
eurjchem-1635	352	4	;	;	PUNCT
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eurjchem-1635	352	6	,	,	PUNCT
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eurjchem-1635	352	8	;	;	PUNCT
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eurjchem-1635	352	10	,	,	PUNCT
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eurjchem-1635	352	12	;	;	PUNCT
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eurjchem-1635	352	14	,	,	PUNCT
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eurjchem-1635	352	16	;	;	PUNCT
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eurjchem-1635	352	18	,	,	PUNCT
eurjchem-1635	352	19	s.	s.	PROPN
eurjchem-1635	352	20	;	;	PUNCT
eurjchem-1635	352	21	bistoni	bistoni	PROPN
eurjchem-1635	352	22	,	,	PUNCT
eurjchem-1635	352	23	f.	f.	PROPN
eurjchem-1635	352	24	;	;	PUNCT
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eurjchem-1635	352	26	,	,	PUNCT
eurjchem-1635	352	27	a.	a.	NOUN
eurjchem-1635	352	28	bioorg	bioorg	PROPN
eurjchem-1635	352	29	.	.	PUNCT
eurjchem-1635	353	1	med	med	PROPN
eurjchem-1635	353	2	.	.	PROPN
eurjchem-1635	353	3	chem	chem	PROPN
eurjchem-1635	353	4	.	.	PUNCT
eurjchem-1635	354	1	2002	2002	NUM
eurjchem-1635	354	2	,	,	PUNCT
eurjchem-1635	354	3	10(6	10(6	NUM
eurjchem-1635	354	4	)	)	PUNCT
eurjchem-1635	354	5	,	,	PUNCT
eurjchem-1635	354	6	1681‐	1681‐	NUM
eurjchem-1635	354	7	1686	1686	NUM
eurjchem-1635	354	8	.	.	PUNCT
eurjchem-1635	355	1	[	[	X
eurjchem-1635	355	2	12	12	NUM
eurjchem-1635	355	3	]	]	PUNCT
eurjchem-1635	355	4	.	.	PUNCT
eurjchem-1635	356	1	fringuelli	fringuelli	PROPN
eurjchem-1635	356	2	,	,	PUNCT
eurjchem-1635	356	3	r.	r.	PROPN
eurjchem-1635	356	4	;	;	PUNCT
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eurjchem-1635	356	6	,	,	PUNCT
eurjchem-1635	356	7	n.	n.	NOUN
eurjchem-1635	356	8	;	;	PUNCT
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eurjchem-1635	356	10	,	,	PUNCT
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eurjchem-1635	356	14	,	,	PUNCT
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eurjchem-1635	356	16	;	;	PUNCT
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eurjchem-1635	356	18	,	,	PUNCT
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eurjchem-1635	356	22	,	,	PUNCT
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eurjchem-1635	356	24	;	;	PUNCT
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eurjchem-1635	356	26	,	,	PUNCT
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eurjchem-1635	356	28	;	;	PUNCT
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eurjchem-1635	356	30	,	,	PUNCT
eurjchem-1635	356	31	f.	f.	PROPN
eurjchem-1635	356	32	bioorg	bioorg	PROPN
eurjchem-1635	356	33	.	.	PUNCT
eurjchem-1635	357	1	med	med	PROPN
eurjchem-1635	357	2	.	.	PUNCT
eurjchem-1635	357	3	chem	chem	PROPN
eurjchem-1635	357	4	.	.	PUNCT
eurjchem-1635	358	1	2009	2009	NUM
eurjchem-1635	358	2	,	,	PUNCT
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eurjchem-1635	358	4	,	,	PUNCT
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eurjchem-1635	358	6	.	.	PUNCT
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eurjchem-1635	359	3	]	]	PUNCT
eurjchem-1635	359	4	.	.	PUNCT
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eurjchem-1635	360	2	,	,	PUNCT
eurjchem-1635	360	3	c.	c.	PROPN
eurjchem-1635	360	4	;	;	PUNCT
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eurjchem-1635	360	6	,	,	PUNCT
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eurjchem-1635	360	8	k.	k.	PROPN
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eurjchem-1635	360	13	;	;	PUNCT
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eurjchem-1635	360	17	j.	j.	PROPN
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eurjchem-1635	360	23	;	;	PUNCT
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eurjchem-1635	360	25	,	,	PUNCT
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eurjchem-1635	360	28	.	.	PUNCT
eurjchem-1635	361	1	j.	j.	PROPN
eurjchem-1635	361	2	med	med	PROPN
eurjchem-1635	361	3	.	.	PROPN
eurjchem-1635	361	4	chem	chem	PROPN
eurjchem-1635	361	5	.	.	PUNCT
eurjchem-1635	362	1	2011	2011	NUM
eurjchem-1635	362	2	,	,	PUNCT
eurjchem-1635	362	3	46	46	NUM
eurjchem-1635	362	4	,	,	PUNCT
eurjchem-1635	362	5	4887‐4896	4887‐4896	NOUN
eurjchem-1635	362	6	.	.	PUNCT
eurjchem-1635	363	1	[	[	X
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eurjchem-1635	363	3	]	]	SYM
eurjchem-1635	363	4	.	.	PUNCT
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eurjchem-1635	364	2	,	,	PUNCT
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eurjchem-1635	364	4	;	;	PUNCT
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eurjchem-1635	364	6	,	,	PUNCT
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eurjchem-1635	364	8	;	;	PUNCT
eurjchem-1635	364	9	aono	aono	PROPN
eurjchem-1635	364	10	,	,	PUNCT
eurjchem-1635	364	11	h.	h.	PROPN
eurjchem-1635	364	12	;	;	PUNCT
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eurjchem-1635	364	16	bioorg	bioorg	PROPN
eurjchem-1635	364	17	.	.	PUNCT
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eurjchem-1635	365	2	.	.	PUNCT
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eurjchem-1635	365	4	.	.	PUNCT
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eurjchem-1635	366	2	,	,	PUNCT
eurjchem-1635	366	3	17	17	NUM
eurjchem-1635	366	4	,	,	PUNCT
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eurjchem-1635	366	6	.	.	PUNCT
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eurjchem-1635	367	2	15	15	NUM
eurjchem-1635	367	3	]	]	PUNCT
eurjchem-1635	367	4	.	.	PUNCT
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eurjchem-1635	368	2	,	,	PUNCT
eurjchem-1635	368	3	t.	t.	PROPN
eurjchem-1635	368	4	;	;	PUNCT
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eurjchem-1635	368	6	,	,	PUNCT
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eurjchem-1635	368	8	;	;	PUNCT
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eurjchem-1635	368	10	,	,	PUNCT
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eurjchem-1635	368	12	;	;	PUNCT
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eurjchem-1635	368	18	,	,	PUNCT
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eurjchem-1635	368	22	,	,	PUNCT
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eurjchem-1635	368	24	;	;	PUNCT
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eurjchem-1635	368	28	;	;	PUNCT
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eurjchem-1635	368	30	,	,	PUNCT
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eurjchem-1635	368	32	;	;	PUNCT
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eurjchem-1635	368	36	;	;	PUNCT
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eurjchem-1635	368	38	,	,	PUNCT
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eurjchem-1635	368	41	;	;	PUNCT
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eurjchem-1635	368	46	;	;	PUNCT
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eurjchem-1635	368	56	;	;	PUNCT
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eurjchem-1635	368	59	s.	s.	PROPN
eurjchem-1635	368	60	a.	a.	PROPN
eurjchem-1635	368	61	;	;	PUNCT
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eurjchem-1635	368	65	bioorg	bioorg	PROPN
eurjchem-1635	368	66	.	.	PUNCT
eurjchem-1635	369	1	med	med	PROPN
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eurjchem-1635	369	4	.	.	PUNCT
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eurjchem-1635	370	2	,	,	PUNCT
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eurjchem-1635	370	4	,	,	PUNCT
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eurjchem-1635	370	6	.	.	PUNCT
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eurjchem-1635	371	2	16	16	NUM
eurjchem-1635	371	3	]	]	PUNCT
eurjchem-1635	371	4	.	.	PUNCT
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eurjchem-1635	372	2	,	,	PUNCT
eurjchem-1635	372	3	k.	k.	PROPN
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eurjchem-1635	372	5	;	;	PUNCT
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eurjchem-1635	372	7	,	,	PUNCT
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eurjchem-1635	372	9	;	;	PUNCT
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eurjchem-1635	372	13	;	;	PUNCT
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eurjchem-1635	372	17	;	;	PUNCT
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eurjchem-1635	372	21	;	;	PUNCT
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eurjchem-1635	372	25	j.	j.	PROPN
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eurjchem-1635	372	27	.	.	PUNCT
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eurjchem-1635	373	4	.	.	PUNCT
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eurjchem-1635	374	2	,	,	PUNCT
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eurjchem-1635	374	6	.	.	PUNCT
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eurjchem-1635	375	4	.	.	PUNCT
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eurjchem-1635	376	2	,	,	PUNCT
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eurjchem-1635	376	8	;	;	PUNCT
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eurjchem-1635	376	21	;	;	PUNCT
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eurjchem-1635	376	31	.	.	PUNCT
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eurjchem-1635	377	4	.	.	PUNCT
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eurjchem-1635	378	2	.	.	PROPN
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eurjchem-1635	379	2	,	,	PUNCT
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eurjchem-1635	380	4	.	.	PUNCT
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eurjchem-1635	381	9	;	;	PUNCT
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eurjchem-1635	381	40	.	.	PUNCT
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eurjchem-1635	386	20	;	;	PUNCT
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