id	sid	tid	token	lemma	pos
eurjchem-170	1	1	untitled	untitle	VERB
eurjchem-170	1	2	european	european	PROPN
eurjchem-170	1	3	journal	journal	PROPN
eurjchem-170	1	4	of	of	ADP
eurjchem-170	1	5	chemistry	chemistry	NOUN
eurjchem-170	1	6	2	2	NUM
eurjchem-170	1	7	(	(	PUNCT
eurjchem-170	1	8	2	2	NUM
eurjchem-170	1	9	)	)	PUNCT
eurjchem-170	1	10	(	(	PUNCT
eurjchem-170	1	11	2011	2011	NUM
eurjchem-170	1	12	)	)	PUNCT
eurjchem-170	1	13	152‐157	152‐157	NUM
eurjchem-170	1	14	european	european	ADJ
eurjchem-170	1	15	journal	journal	PROPN
eurjchem-170	1	16	of	of	ADP
eurjchem-170	1	17	chemistry	chemistry	NOUN
eurjchem-170	1	18	issn	issn	PROPN
eurjchem-170	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-170	1	20	(	(	PUNCT
eurjchem-170	1	21	print	print	NOUN
eurjchem-170	1	22	)	)	PUNCT
eurjchem-170	1	23	/	/	SYM
eurjchem-170	1	24	issn	issn	PROPN
eurjchem-170	1	25	2153‐2257	2153‐2257	NUM
eurjchem-170	1	26	(	(	PUNCT
eurjchem-170	1	27	online	online	ADJ
eurjchem-170	1	28	)	)	PUNCT
eurjchem-170	1	29			NOUN
eurjchem-170	1	30	2011	2011	NUM
eurjchem-170	1	31	eurjchem	eurjchem	PROPN
eurjchem-170	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-170	1	33	/	/	SYM
eurjchem-170	1	34	eurjchem.2.2.152‐157.170	eurjchem.2.2.152‐157.170	ADJ
eurjchem-170	1	35	european	european	PROPN
eurjchem-170	1	36	journal	journal	PROPN
eurjchem-170	1	37	of	of	ADP
eurjchem-170	1	38	chemistry	chemistry	PROPN
eurjchem-170	1	39	journal	journal	PROPN
eurjchem-170	1	40	homepage	homepage	NOUN
eurjchem-170	1	41	:	:	PUNCT
eurjchem-170	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-170	1	43	identification	identification	NOUN
eurjchem-170	1	44	and	and	CCONJ
eurjchem-170	1	45	characterization	characterization	NOUN
eurjchem-170	1	46	of	of	ADP
eurjchem-170	1	47	geometrical	geometrical	ADJ
eurjchem-170	1	48	isomeric	isomeric	ADJ
eurjchem-170	1	49	photo	photo	NOUN
eurjchem-170	1	50	degradation	degradation	NOUN
eurjchem-170	1	51	product	product	NOUN
eurjchem-170	1	52	of	of	ADP
eurjchem-170	1	53	eprosartan	eprosartan	PROPN
eurjchem-170	1	54	using	use	VERB
eurjchem-170	1	55	lc‐ms	lc‐ms	PROPN
eurjchem-170	1	56	and	and	CCONJ
eurjchem-170	1	57	lc‐nmr	lc‐nmr	PROPN
eurjchem-170	1	58	ravi	ravi	PROPN
eurjchem-170	1	59	piyushkumar	piyushkumar	ADJ
eurjchem-170	1	60	shah	shah	NOUN
eurjchem-170	1	61	,	,	PUNCT
eurjchem-170	1	62	archana	archana	PROPN
eurjchem-170	1	63	sahu	sahu	PROPN
eurjchem-170	1	64	and	and	CCONJ
eurjchem-170	1	65	saranjit	saranjit	PROPN
eurjchem-170	1	66	singh	singh	PROPN
eurjchem-170	1	67	*	*	PROPN
eurjchem-170	1	68	department	department	PROPN
eurjchem-170	1	69	of	of	ADP
eurjchem-170	1	70	pharmaceutical	pharmaceutical	ADJ
eurjchem-170	1	71	analysis	analysis	NOUN
eurjchem-170	1	72	,	,	PUNCT
eurjchem-170	1	73	national	national	PROPN
eurjchem-170	1	74	institute	institute	PROPN
eurjchem-170	1	75	of	of	ADP
eurjchem-170	1	76	pharmaceutical	pharmaceutical	NOUN
eurjchem-170	1	77	education	education	NOUN
eurjchem-170	1	78	and	and	CCONJ
eurjchem-170	1	79	research	research	NOUN
eurjchem-170	1	80	(	(	PUNCT
eurjchem-170	1	81	niper	niper	NOUN
eurjchem-170	1	82	)	)	PUNCT
eurjchem-170	1	83	,	,	PUNCT
eurjchem-170	1	84	sas	sa	VERB
eurjchem-170	1	85	nagar	nagar	NOUN
eurjchem-170	1	86	160062	160062	NUM
eurjchem-170	1	87	,	,	PUNCT
eurjchem-170	1	88	punjab	punjab	PROPN
eurjchem-170	1	89	,	,	PUNCT
eurjchem-170	1	90	india	india	PROPN
eurjchem-170	1	91	*	*	PUNCT
eurjchem-170	1	92	corresponding	correspond	VERB
eurjchem-170	1	93	author	author	NOUN
eurjchem-170	1	94	at	at	ADP
eurjchem-170	1	95	:	:	PUNCT
eurjchem-170	1	96	department	department	NOUN
eurjchem-170	1	97	of	of	ADP
eurjchem-170	1	98	pharmaceutical	pharmaceutical	ADJ
eurjchem-170	1	99	analysis	analysis	NOUN
eurjchem-170	1	100	,	,	PUNCT
eurjchem-170	1	101	national	national	PROPN
eurjchem-170	1	102	institute	institute	PROPN
eurjchem-170	1	103	of	of	ADP
eurjchem-170	1	104	pharmaceutical	pharmaceutical	NOUN
eurjchem-170	1	105	education	education	NOUN
eurjchem-170	1	106	and	and	CCONJ
eurjchem-170	1	107	research	research	NOUN
eurjchem-170	1	108	(	(	PUNCT
eurjchem-170	1	109	niper	niper	NOUN
eurjchem-170	1	110	)	)	PUNCT
eurjchem-170	1	111	,	,	PUNCT
eurjchem-170	1	112	sahibzada	sahibzada	PROPN
eurjchem-170	1	113	ajit	ajit	PROPN
eurjchem-170	1	114	singh	singh	PROPN
eurjchem-170	1	115	,	,	PUNCT
eurjchem-170	1	116	nagar	nagar	NOUN
eurjchem-170	1	117	160062	160062	NUM
eurjchem-170	1	118	,	,	PUNCT
eurjchem-170	1	119	punjab	punjab	PROPN
eurjchem-170	1	120	,	,	PUNCT
eurjchem-170	1	121	india	india	PROPN
eurjchem-170	1	122	.	.	PUNCT
eurjchem-170	2	1	tel	tel	PROPN
eurjchem-170	2	2	.	.	PUNCT
eurjchem-170	2	3	:	:	PUNCT
eurjchem-170	3	1	+91.172.2214682	+91.172.2214682	ADV
eurjchem-170	3	2	;	;	PUNCT
eurjchem-170	3	3	fax	fax	NOUN
eurjchem-170	3	4	:	:	PUNCT
eurjchem-170	3	5	+91.172.2214692	+91.172.2214692	NUM
eurjchem-170	3	6	.	.	PUNCT
eurjchem-170	3	7	e‐mail	e‐mail	PUNCT
eurjchem-170	3	8	address	address	NOUN
eurjchem-170	3	9	:	:	PUNCT
eurjchem-170	3	10	ssingh@niper.ac.in	ssingh@niper.ac.in	PROPN
eurjchem-170	3	11	(	(	PUNCT
eurjchem-170	3	12	s.	s.	PROPN
eurjchem-170	3	13	singh	singh	PROPN
eurjchem-170	3	14	)	)	PUNCT
eurjchem-170	3	15	.	.	PUNCT
eurjchem-170	4	1	communication	communication	NOUN
eurjchem-170	4	2	information	information	NOUN
eurjchem-170	4	3	abstract	abstract	ADJ
eurjchem-170	4	4	received	receive	VERB
eurjchem-170	4	5	:	:	PUNCT
eurjchem-170	4	6	17	17	NUM
eurjchem-170	4	7	june	june	PROPN
eurjchem-170	4	8	2010	2010	NUM
eurjchem-170	4	9	received	receive	VERB
eurjchem-170	4	10	in	in	ADP
eurjchem-170	4	11	revised	revise	VERB
eurjchem-170	4	12	form	form	NOUN
eurjchem-170	4	13	:	:	PUNCT
eurjchem-170	4	14	02	02	NUM
eurjchem-170	4	15	november	november	PROPN
eurjchem-170	4	16	2010	2010	NUM
eurjchem-170	4	17	accepted	accept	VERB
eurjchem-170	4	18	:	:	PUNCT
eurjchem-170	4	19	02	02	NUM
eurjchem-170	4	20	november	november	PROPN
eurjchem-170	4	21	2010	2010	NUM
eurjchem-170	4	22	online	online	NOUN
eurjchem-170	4	23	:	:	PUNCT
eurjchem-170	4	24	30	30	NUM
eurjchem-170	4	25	june	june	PROPN
eurjchem-170	4	26	2011	2011	NUM
eurjchem-170	4	27	keywords	keyword	VERB
eurjchem-170	4	28	the	the	DET
eurjchem-170	4	29	degradation	degradation	NOUN
eurjchem-170	4	30	of	of	ADP
eurjchem-170	4	31	eprosartan	eprosartan	PROPN
eurjchem-170	4	32	was	be	AUX
eurjchem-170	4	33	evaluated	evaluate	VERB
eurjchem-170	4	34	under	under	ADP
eurjchem-170	4	35	ich	ich	PROPN
eurjchem-170	4	36	/	/	SYM
eurjchem-170	4	37	who	who	PRON
eurjchem-170	4	38	prescribed	prescribe	VERB
eurjchem-170	4	39	stress	stress	NOUN
eurjchem-170	4	40	conditions	condition	NOUN
eurjchem-170	4	41	.	.	PUNCT
eurjchem-170	5	1	the	the	DET
eurjchem-170	5	2	drug	drug	NOUN
eurjchem-170	5	3	degraded	degrade	VERB
eurjchem-170	5	4	to	to	ADP
eurjchem-170	5	5	only	only	ADV
eurjchem-170	5	6	one	one	NUM
eurjchem-170	5	7	product	product	NOUN
eurjchem-170	5	8	under	under	ADP
eurjchem-170	5	9	photo	photo	NOUN
eurjchem-170	5	10	alkali	alkali	ADJ
eurjchem-170	5	11	condition	condition	NOUN
eurjchem-170	5	12	,	,	PUNCT
eurjchem-170	5	13	whereas	whereas	SCONJ
eurjchem-170	5	14	it	it	PRON
eurjchem-170	5	15	was	be	AUX
eurjchem-170	5	16	stable	stable	ADJ
eurjchem-170	5	17	to	to	ADP
eurjchem-170	5	18	conditions	condition	NOUN
eurjchem-170	5	19	of	of	ADP
eurjchem-170	5	20	hydrolysis	hydrolysis	NOUN
eurjchem-170	5	21	,	,	PUNCT
eurjchem-170	5	22	oxidation	oxidation	NOUN
eurjchem-170	5	23	and	and	CCONJ
eurjchem-170	5	24	thermal	thermal	ADJ
eurjchem-170	5	25	stress	stress	NOUN
eurjchem-170	5	26	.	.	PUNCT
eurjchem-170	6	1	the	the	DET
eurjchem-170	6	2	drug	drug	NOUN
eurjchem-170	6	3	and	and	CCONJ
eurjchem-170	6	4	its	its	PRON
eurjchem-170	6	5	co‐eluting	co‐eluting	NOUN
eurjchem-170	6	6	product	product	NOUN
eurjchem-170	6	7	were	be	AUX
eurjchem-170	6	8	well	well	ADV
eurjchem-170	6	9	separated	separate	VERB
eurjchem-170	6	10	on	on	ADP
eurjchem-170	6	11	rp‐hplc	rp‐hplc	PROPN
eurjchem-170	6	12	in	in	ADP
eurjchem-170	6	13	a	a	DET
eurjchem-170	6	14	gradient	gradient	ADJ
eurjchem-170	6	15	mode	mode	NOUN
eurjchem-170	6	16	.	.	PUNCT
eurjchem-170	7	1	subsequently	subsequently	ADV
eurjchem-170	7	2	,	,	PUNCT
eurjchem-170	7	3	lc‐ms	lc‐ms	AUX
eurjchem-170	7	4	/	/	SYM
eurjchem-170	7	5	tof	tof	PROPN
eurjchem-170	7	6	and	and	CCONJ
eurjchem-170	7	7	on‐line	on‐line	PROPN
eurjchem-170	7	8	h	h	NOUN
eurjchem-170	7	9	/	/	SYM
eurjchem-170	7	10	d	d	NOUN
eurjchem-170	7	11	exchange	exchange	NOUN
eurjchem-170	7	12	studies	study	NOUN
eurjchem-170	7	13	were	be	AUX
eurjchem-170	7	14	performed	perform	VERB
eurjchem-170	7	15	on	on	ADP
eurjchem-170	7	16	both	both	PRON
eurjchem-170	7	17	of	of	ADP
eurjchem-170	7	18	them	they	PRON
eurjchem-170	7	19	.	.	PUNCT
eurjchem-170	8	1	the	the	DET
eurjchem-170	8	2	two	two	NUM
eurjchem-170	8	3	showed	show	VERB
eurjchem-170	8	4	same	same	ADJ
eurjchem-170	8	5	molecular	molecular	ADJ
eurjchem-170	8	6	mass	mass	NOUN
eurjchem-170	8	7	,	,	PUNCT
eurjchem-170	8	8	similar	similar	ADJ
eurjchem-170	8	9	fragment	fragment	ADJ
eurjchem-170	8	10	ions	ion	NOUN
eurjchem-170	8	11	and	and	CCONJ
eurjchem-170	8	12	even	even	ADV
eurjchem-170	8	13	the	the	DET
eurjchem-170	8	14	same	same	ADJ
eurjchem-170	8	15	number	number	NOUN
eurjchem-170	8	16	of	of	ADP
eurjchem-170	8	17	labile	labile	ADJ
eurjchem-170	8	18	hydrogens	hydrogen	NOUN
eurjchem-170	8	19	indicating	indicate	VERB
eurjchem-170	8	20	the	the	DET
eurjchem-170	8	21	product	product	NOUN
eurjchem-170	8	22	to	to	PART
eurjchem-170	8	23	be	be	AUX
eurjchem-170	8	24	an	an	DET
eurjchem-170	8	25	isomer	isomer	NOUN
eurjchem-170	8	26	of	of	ADP
eurjchem-170	8	27	the	the	DET
eurjchem-170	8	28	drug	drug	NOUN
eurjchem-170	8	29	.	.	PUNCT
eurjchem-170	9	1	to	to	PART
eurjchem-170	9	2	confirm	confirm	VERB
eurjchem-170	9	3	the	the	DET
eurjchem-170	9	4	same	same	ADJ
eurjchem-170	9	5	,	,	PUNCT
eurjchem-170	9	6	1h	1h	NUM
eurjchem-170	9	7	and	and	CCONJ
eurjchem-170	9	8	cosy	cosy	PROPN
eurjchem-170	9	9	lc‐nmr	lc‐nmr	PROPN
eurjchem-170	9	10	studies	study	NOUN
eurjchem-170	9	11	were	be	AUX
eurjchem-170	9	12	carried	carry	VERB
eurjchem-170	9	13	out	out	ADP
eurjchem-170	9	14	by	by	ADP
eurjchem-170	9	15	using	use	VERB
eurjchem-170	9	16	an	an	DET
eurjchem-170	9	17	enriched	enriched	ADJ
eurjchem-170	9	18	sample	sample	NOUN
eurjchem-170	9	19	.	.	PUNCT
eurjchem-170	10	1	distinguishing	distinguish	VERB
eurjchem-170	10	2	behaviour	behaviour	NOUN
eurjchem-170	10	3	of	of	ADP
eurjchem-170	10	4	chemical	chemical	ADJ
eurjchem-170	10	5	shifts	shift	NOUN
eurjchem-170	10	6	proved	prove	VERB
eurjchem-170	10	7	the	the	DET
eurjchem-170	10	8	product	product	NOUN
eurjchem-170	10	9	to	to	PART
eurjchem-170	10	10	be	be	AUX
eurjchem-170	10	11	(	(	PUNCT
eurjchem-170	10	12	z)‐4‐((2‐butyl‐5‐(2‐carboxy‐3‐(thiophen‐2‐yl)prop‐1‐enyl)‐1h‐imidazol‐1‐	z)‐4‐((2‐butyl‐5‐(2‐carboxy‐3‐(thiophen‐2‐yl)prop‐1‐enyl)‐1h‐imidazol‐1‐	X
eurjchem-170	10	13	yl)methyl)benzoic	yl)methyl)benzoic	NUM
eurjchem-170	10	14	acid	acid	NOUN
eurjchem-170	10	15	.	.	PUNCT
eurjchem-170	11	1	the	the	DET
eurjchem-170	11	2	structure	structure	NOUN
eurjchem-170	11	3	was	be	AUX
eurjchem-170	11	4	further	far	ADV
eurjchem-170	11	5	supported	support	VERB
eurjchem-170	11	6	by	by	ADP
eurjchem-170	11	7	differential	differential	ADJ
eurjchem-170	11	8	lc‐ms	lc‐ms	PROPN
eurjchem-170	11	9	ion	ion	NOUN
eurjchem-170	11	10	intensities	intensity	NOUN
eurjchem-170	11	11	of	of	ADP
eurjchem-170	11	12	the	the	DET
eurjchem-170	11	13	drug	drug	NOUN
eurjchem-170	11	14	and	and	CCONJ
eurjchem-170	11	15	the	the	DET
eurjchem-170	11	16	product	product	NOUN
eurjchem-170	11	17	.	.	PUNCT
eurjchem-170	12	1	eprosartan	eprosartan	PROPN
eurjchem-170	12	2	degradation	degradation	PROPN
eurjchem-170	12	3	behaviour	behaviour	NOUN
eurjchem-170	12	4	photoisomerization	photoisomerization	NOUN
eurjchem-170	12	5	geometric	geometric	ADJ
eurjchem-170	12	6	isomer	isomer	PROPN
eurjchem-170	12	7	lc‐ms	lc‐ms	AUX
eurjchem-170	12	8	lc‐nmr	lc‐nmr	PROPN
eurjchem-170	12	9	1	1	NUM
eurjchem-170	12	10	.	.	PUNCT
eurjchem-170	12	11	introduction	introduction	NOUN
eurjchem-170	12	12	as	as	ADP
eurjchem-170	12	13	per	per	ADP
eurjchem-170	12	14	the	the	DET
eurjchem-170	12	15	international	international	ADJ
eurjchem-170	12	16	conference	conference	NOUN
eurjchem-170	12	17	on	on	ADP
eurjchem-170	12	18	harmonization	harmonization	NOUN
eurjchem-170	12	19	(	(	PUNCT
eurjchem-170	12	20	ich	ich	NOUN
eurjchem-170	12	21	)	)	PUNCT
eurjchem-170	13	1	[	[	X
eurjchem-170	13	2	1	1	X
eurjchem-170	13	3	]	]	PUNCT
eurjchem-170	13	4	and	and	CCONJ
eurjchem-170	13	5	the	the	DET
eurjchem-170	13	6	world	world	PROPN
eurjchem-170	13	7	health	health	NOUN
eurjchem-170	13	8	organization	organization	NOUN
eurjchem-170	13	9	(	(	PUNCT
eurjchem-170	13	10	who	who	PRON
eurjchem-170	13	11	)	)	PUNCT
eurjchem-170	14	1	[	[	X
eurjchem-170	14	2	2	2	NUM
eurjchem-170	14	3	]	]	PUNCT
eurjchem-170	14	4	stability	stability	NOUN
eurjchem-170	14	5	test	test	NOUN
eurjchem-170	14	6	guidelines	guideline	NOUN
eurjchem-170	14	7	,	,	PUNCT
eurjchem-170	14	8	stress	stress	NOUN
eurjchem-170	14	9	studies	study	NOUN
eurjchem-170	14	10	and	and	CCONJ
eurjchem-170	14	11	identification/	identification/	NUM
eurjchem-170	14	12	characterization	characterization	NOUN
eurjchem-170	14	13	of	of	ADP
eurjchem-170	14	14	degradation	degradation	NOUN
eurjchem-170	14	15	product(s	product(s	NOUN
eurjchem-170	14	16	)	)	PUNCT
eurjchem-170	14	17	are	be	AUX
eurjchem-170	14	18	mandatory	mandatory	ADJ
eurjchem-170	14	19	for	for	ADP
eurjchem-170	14	20	new	new	ADJ
eurjchem-170	14	21	and	and	CCONJ
eurjchem-170	14	22	existing	exist	VERB
eurjchem-170	14	23	drug	drug	NOUN
eurjchem-170	14	24	molecules	molecule	NOUN
eurjchem-170	14	25	,	,	PUNCT
eurjchem-170	14	26	respectively	respectively	ADV
eurjchem-170	14	27	.	.	PUNCT
eurjchem-170	15	1	generally	generally	ADV
eurjchem-170	15	2	during	during	ADP
eurjchem-170	15	3	stress	stress	NOUN
eurjchem-170	15	4	and	and	CCONJ
eurjchem-170	15	5	stability	stability	NOUN
eurjchem-170	15	6	studies	study	NOUN
eurjchem-170	15	7	,	,	PUNCT
eurjchem-170	15	8	the	the	DET
eurjchem-170	15	9	degradation	degradation	NOUN
eurjchem-170	15	10	products	product	NOUN
eurjchem-170	15	11	are	be	AUX
eurjchem-170	15	12	generated	generate	VERB
eurjchem-170	15	13	in	in	ADP
eurjchem-170	15	14	small	small	ADJ
eurjchem-170	15	15	quantities	quantity	NOUN
eurjchem-170	15	16	.	.	PUNCT
eurjchem-170	16	1	so	so	ADV
eurjchem-170	16	2	their	their	PRON
eurjchem-170	16	3	characterization	characterization	NOUN
eurjchem-170	16	4	turns	turn	VERB
eurjchem-170	16	5	out	out	ADP
eurjchem-170	16	6	to	to	PART
eurjchem-170	16	7	be	be	AUX
eurjchem-170	16	8	a	a	DET
eurjchem-170	16	9	cumbersome	cumbersome	ADJ
eurjchem-170	16	10	process	process	NOUN
eurjchem-170	16	11	,	,	PUNCT
eurjchem-170	16	12	when	when	SCONJ
eurjchem-170	16	13	the	the	DET
eurjchem-170	16	14	conventional	conventional	ADJ
eurjchem-170	16	15	approach	approach	NOUN
eurjchem-170	16	16	of	of	ADP
eurjchem-170	16	17	isolation	isolation	NOUN
eurjchem-170	16	18	and	and	CCONJ
eurjchem-170	16	19	spectral	spectral	ADJ
eurjchem-170	16	20	analysis	analysis	NOUN
eurjchem-170	16	21	is	be	AUX
eurjchem-170	16	22	followed	follow	VERB
eurjchem-170	16	23	.	.	PUNCT
eurjchem-170	17	1	therefore	therefore	ADV
eurjchem-170	17	2	,	,	PUNCT
eurjchem-170	17	3	advanced	advance	VERB
eurjchem-170	17	4	hyphenated	hyphenated	ADJ
eurjchem-170	17	5	techniques	technique	NOUN
eurjchem-170	17	6	,	,	PUNCT
eurjchem-170	17	7	like	like	ADP
eurjchem-170	17	8	lc‐ms	lc‐ms	NOUN
eurjchem-170	17	9	and	and	CCONJ
eurjchem-170	17	10	lc‐nmr	lc‐nmr	PROPN
eurjchem-170	17	11	,	,	PUNCT
eurjchem-170	17	12	are	be	AUX
eurjchem-170	17	13	being	be	AUX
eurjchem-170	17	14	extensively	extensively	ADV
eurjchem-170	17	15	explored	explore	VERB
eurjchem-170	17	16	for	for	ADP
eurjchem-170	17	17	this	this	DET
eurjchem-170	17	18	purpose	purpose	NOUN
eurjchem-170	17	19	since	since	SCONJ
eurjchem-170	17	20	the	the	DET
eurjchem-170	17	21	last	last	ADJ
eurjchem-170	17	22	few	few	ADJ
eurjchem-170	17	23	years	year	NOUN
eurjchem-170	18	1	[	[	X
eurjchem-170	18	2	3‐8	3‐8	NOUN
eurjchem-170	18	3	]	]	X
eurjchem-170	18	4	.	.	PUNCT
eurjchem-170	19	1	eprosartan	eprosartan	PROPN
eurjchem-170	19	2	is	be	AUX
eurjchem-170	19	3	an	an	DET
eurjchem-170	19	4	angiotensin	angiotensin	NOUN
eurjchem-170	19	5	ii	ii	NOUN
eurjchem-170	19	6	receptor	receptor	NOUN
eurjchem-170	19	7	antagonist	antagonist	NOUN
eurjchem-170	19	8	,	,	PUNCT
eurjchem-170	19	9	which	which	PRON
eurjchem-170	19	10	is	be	AUX
eurjchem-170	19	11	used	use	VERB
eurjchem-170	19	12	in	in	ADP
eurjchem-170	19	13	the	the	DET
eurjchem-170	19	14	treatment	treatment	NOUN
eurjchem-170	19	15	of	of	ADP
eurjchem-170	19	16	hypertension	hypertension	NOUN
eurjchem-170	19	17	[	[	X
eurjchem-170	19	18	9	9	NUM
eurjchem-170	19	19	]	]	PUNCT
eurjchem-170	19	20	.	.	PUNCT
eurjchem-170	20	1	although	although	SCONJ
eurjchem-170	20	2	,	,	PUNCT
eurjchem-170	20	3	the	the	DET
eurjchem-170	20	4	drug	drug	NOUN
eurjchem-170	20	5	was	be	AUX
eurjchem-170	20	6	approved	approve	VERB
eurjchem-170	20	7	by	by	ADP
eurjchem-170	20	8	us‐fda	us‐fda	PROPN
eurjchem-170	20	9	in	in	ADP
eurjchem-170	20	10	1997	1997	NUM
eurjchem-170	20	11	[	[	X
eurjchem-170	20	12	10	10	NUM
eurjchem-170	20	13	]	]	PUNCT
eurjchem-170	20	14	,	,	PUNCT
eurjchem-170	20	15	only	only	ADV
eurjchem-170	20	16	scant	scant	ADJ
eurjchem-170	20	17	information	information	NOUN
eurjchem-170	20	18	on	on	ADP
eurjchem-170	20	19	its	its	PRON
eurjchem-170	20	20	degradation	degradation	NOUN
eurjchem-170	20	21	behaviour	behaviour	NOUN
eurjchem-170	20	22	is	be	AUX
eurjchem-170	20	23	known	know	VERB
eurjchem-170	20	24	[	[	PUNCT
eurjchem-170	20	25	11	11	NUM
eurjchem-170	20	26	]	]	PUNCT
eurjchem-170	20	27	.	.	PUNCT
eurjchem-170	21	1	there	there	PRON
eurjchem-170	21	2	is	be	VERB
eurjchem-170	21	3	no	no	DET
eurjchem-170	21	4	report	report	NOUN
eurjchem-170	21	5	involving	involve	VERB
eurjchem-170	21	6	stress	stress	NOUN
eurjchem-170	21	7	testing	testing	NOUN
eurjchem-170	21	8	on	on	ADP
eurjchem-170	21	9	the	the	DET
eurjchem-170	21	10	drug	drug	NOUN
eurjchem-170	21	11	.	.	PUNCT
eurjchem-170	22	1	most	most	ADJ
eurjchem-170	22	2	of	of	ADP
eurjchem-170	22	3	the	the	DET
eurjchem-170	22	4	literature	literature	NOUN
eurjchem-170	22	5	texts	text	NOUN
eurjchem-170	22	6	cover	cover	VERB
eurjchem-170	22	7	development	development	NOUN
eurjchem-170	22	8	of	of	ADP
eurjchem-170	22	9	hplc	hplc	NOUN
eurjchem-170	22	10	and	and	CCONJ
eurjchem-170	22	11	lc‐ms	lc‐ms	NOUN
eurjchem-170	22	12	methods	method	NOUN
eurjchem-170	22	13	for	for	ADP
eurjchem-170	22	14	the	the	DET
eurjchem-170	22	15	determination	determination	NOUN
eurjchem-170	22	16	of	of	ADP
eurjchem-170	22	17	drug	drug	NOUN
eurjchem-170	22	18	in	in	ADP
eurjchem-170	22	19	different	different	ADJ
eurjchem-170	22	20	matrices	matrix	NOUN
eurjchem-170	22	21	[	[	X
eurjchem-170	22	22	11‐13	11‐13	NUM
eurjchem-170	22	23	]	]	PUNCT
eurjchem-170	22	24	.	.	PUNCT
eurjchem-170	23	1	therefore	therefore	ADV
eurjchem-170	23	2	,	,	PUNCT
eurjchem-170	23	3	an	an	DET
eurjchem-170	23	4	endeavour	endeavour	NOUN
eurjchem-170	23	5	of	of	ADP
eurjchem-170	23	6	the	the	DET
eurjchem-170	23	7	present	present	ADJ
eurjchem-170	23	8	study	study	NOUN
eurjchem-170	23	9	was	be	AUX
eurjchem-170	23	10	to	to	PART
eurjchem-170	23	11	:	:	PUNCT
eurjchem-170	23	12	(	(	PUNCT
eurjchem-170	23	13	i	i	NOUN
eurjchem-170	23	14	)	)	PUNCT
eurjchem-170	23	15	degrade	degrade	VERB
eurjchem-170	23	16	the	the	DET
eurjchem-170	23	17	drug	drug	NOUN
eurjchem-170	23	18	under	under	ADP
eurjchem-170	23	19	conditions	condition	NOUN
eurjchem-170	23	20	of	of	ADP
eurjchem-170	23	21	hydrolysis	hydrolysis	NOUN
eurjchem-170	23	22	,	,	PUNCT
eurjchem-170	23	23	oxidation	oxidation	NOUN
eurjchem-170	23	24	,	,	PUNCT
eurjchem-170	23	25	photolysis	photolysis	NOUN
eurjchem-170	23	26	and	and	CCONJ
eurjchem-170	23	27	thermal	thermal	ADJ
eurjchem-170	23	28	stress	stress	NOUN
eurjchem-170	23	29	,	,	PUNCT
eurjchem-170	23	30	as	as	SCONJ
eurjchem-170	23	31	prescribed	prescribe	VERB
eurjchem-170	23	32	by	by	ADP
eurjchem-170	23	33	ich	ich	NOUN
eurjchem-170	23	34	and	and	CCONJ
eurjchem-170	23	35	who	who	PRON
eurjchem-170	23	36	,	,	PUNCT
eurjchem-170	23	37	(	(	PUNCT
eurjchem-170	23	38	ii	ii	NOUN
eurjchem-170	23	39	)	)	PUNCT
eurjchem-170	23	40	separate	separate	VERB
eurjchem-170	23	41	the	the	DET
eurjchem-170	23	42	drug	drug	NOUN
eurjchem-170	23	43	and	and	CCONJ
eurjchem-170	23	44	the	the	DET
eurjchem-170	23	45	degradation	degradation	NOUN
eurjchem-170	23	46	product(s	product(s	NOUN
eurjchem-170	23	47	)	)	PUNCT
eurjchem-170	23	48	on	on	ADP
eurjchem-170	23	49	a	a	DET
eurjchem-170	23	50	lc	lc	NOUN
eurjchem-170	23	51	column	column	NOUN
eurjchem-170	23	52	,	,	PUNCT
eurjchem-170	23	53	(	(	PUNCT
eurjchem-170	23	54	iii	iii	NOUN
eurjchem-170	23	55	)	)	PUNCT
eurjchem-170	23	56	obtain	obtain	VERB
eurjchem-170	23	57	necessary	necessary	ADJ
eurjchem-170	23	58	spectral	spectral	ADJ
eurjchem-170	23	59	information	information	NOUN
eurjchem-170	23	60	for	for	ADP
eurjchem-170	23	61	the	the	DET
eurjchem-170	23	62	generated	generate	VERB
eurjchem-170	23	63	degradation	degradation	NOUN
eurjchem-170	23	64	product(s	product(s	NOUN
eurjchem-170	23	65	)	)	PUNCT
eurjchem-170	23	66	using	use	VERB
eurjchem-170	23	67	lc‐ms	lc‐ms	PRON
eurjchem-170	23	68	and	and	CCONJ
eurjchem-170	23	69	lc‐nmr	lc‐nmr	PROPN
eurjchem-170	23	70	,	,	PUNCT
eurjchem-170	23	71	and	and	CCONJ
eurjchem-170	23	72	(	(	PUNCT
eurjchem-170	23	73	iv	iv	X
eurjchem-170	23	74	)	)	PUNCT
eurjchem-170	23	75	characterize	characterize	VERB
eurjchem-170	23	76	the	the	DET
eurjchem-170	23	77	degradation	degradation	NOUN
eurjchem-170	23	78	product(s	product(s	NOUN
eurjchem-170	23	79	)	)	PUNCT
eurjchem-170	23	80	formed	form	VERB
eurjchem-170	23	81	from	from	ADP
eurjchem-170	23	82	the	the	DET
eurjchem-170	23	83	available	available	ADJ
eurjchem-170	23	84	data	datum	NOUN
eurjchem-170	23	85	.	.	PUNCT
eurjchem-170	24	1	2	2	X
eurjchem-170	24	2	.	.	X
eurjchem-170	24	3	experimental	experimental	ADJ
eurjchem-170	24	4	2.1	2.1	NUM
eurjchem-170	24	5	.	.	PUNCT
eurjchem-170	24	6	drug	drug	NOUN
eurjchem-170	24	7	and	and	CCONJ
eurjchem-170	24	8	reagents	reagent	NOUN
eurjchem-170	24	9	pure	pure	ADJ
eurjchem-170	24	10	eprosartan	eprosartan	PROPN
eurjchem-170	24	11	was	be	AUX
eurjchem-170	24	12	obtained	obtain	VERB
eurjchem-170	24	13	as	as	ADP
eurjchem-170	24	14	gratis	gratis	NOUN
eurjchem-170	24	15	sample	sample	NOUN
eurjchem-170	24	16	from	from	ADP
eurjchem-170	24	17	ranbaxy	ranbaxy	PROPN
eurjchem-170	24	18	research	research	NOUN
eurjchem-170	24	19	laboratories	laboratory	NOUN
eurjchem-170	24	20	(	(	PUNCT
eurjchem-170	24	21	gurgaon	gurgaon	PROPN
eurjchem-170	24	22	,	,	PUNCT
eurjchem-170	24	23	india	india	PROPN
eurjchem-170	24	24	)	)	PUNCT
eurjchem-170	24	25	.	.	PUNCT
eurjchem-170	25	1	analytical	analytical	ADJ
eurjchem-170	25	2	reagent	reagent	NOUN
eurjchem-170	25	3	(	(	PUNCT
eurjchem-170	25	4	ar	ar	NOUN
eurjchem-170	25	5	)	)	PUNCT
eurjchem-170	25	6	grade	grade	NOUN
eurjchem-170	25	7	sodium	sodium	NOUN
eurjchem-170	25	8	hydroxide	hydroxide	NOUN
eurjchem-170	25	9	(	(	PUNCT
eurjchem-170	25	10	naoh	naoh	PROPN
eurjchem-170	25	11	)	)	PUNCT
eurjchem-170	25	12	was	be	AUX
eurjchem-170	25	13	purchased	purchase	VERB
eurjchem-170	25	14	from	from	ADP
eurjchem-170	25	15	ranbaxy	ranbaxy	PROPN
eurjchem-170	25	16	laboratories	laboratory	NOUN
eurjchem-170	25	17	(	(	PUNCT
eurjchem-170	25	18	s.a.s	s.a.s	PROPN
eurjchem-170	25	19	.	.	PROPN
eurjchem-170	25	20	nagar	nagar	PROPN
eurjchem-170	25	21	,	,	PUNCT
eurjchem-170	25	22	india	india	PROPN
eurjchem-170	25	23	)	)	PUNCT
eurjchem-170	25	24	,	,	PUNCT
eurjchem-170	25	25	hydrochloric	hydrochloric	ADJ
eurjchem-170	25	26	acid	acid	NOUN
eurjchem-170	25	27	(	(	PUNCT
eurjchem-170	25	28	hcl	hcl	PROPN
eurjchem-170	25	29	)	)	PUNCT
eurjchem-170	25	30	from	from	ADP
eurjchem-170	25	31	loba	loba	PROPN
eurjchem-170	25	32	chemie	chemie	PROPN
eurjchem-170	25	33	pvt	pvt	PROPN
eurjchem-170	25	34	.	.	PROPN
eurjchem-170	25	35	ltd	ltd	PROPN
eurjchem-170	25	36	.	.	PROPN
eurjchem-170	25	37	(	(	PUNCT
eurjchem-170	25	38	mumbai	mumbai	PROPN
eurjchem-170	25	39	,	,	PUNCT
eurjchem-170	25	40	india	india	PROPN
eurjchem-170	25	41	)	)	PUNCT
eurjchem-170	25	42	and	and	CCONJ
eurjchem-170	25	43	hydrogen	hydrogen	NOUN
eurjchem-170	25	44	peroxide	peroxide	NOUN
eurjchem-170	25	45	(	(	PUNCT
eurjchem-170	25	46	h2o2	h2o2	NOUN
eurjchem-170	25	47	)	)	PUNCT
eurjchem-170	25	48	from	from	ADP
eurjchem-170	25	49	s.d	s.d	PROPN
eurjchem-170	25	50	.	.	PROPN
eurjchem-170	25	51	fine‐chem	fine‐chem	PROPN
eurjchem-170	25	52	ltd	ltd	PROPN
eurjchem-170	25	53	.	.	PROPN
eurjchem-170	25	54	(	(	PUNCT
eurjchem-170	25	55	boisar	boisar	PROPN
eurjchem-170	25	56	,	,	PUNCT
eurjchem-170	25	57	india	india	PROPN
eurjchem-170	25	58	)	)	PUNCT
eurjchem-170	25	59	.	.	PUNCT
eurjchem-170	26	1	buffer	buffer	NOUN
eurjchem-170	26	2	salts	salt	NOUN
eurjchem-170	26	3	and	and	CCONJ
eurjchem-170	26	4	all	all	DET
eurjchem-170	26	5	other	other	ADJ
eurjchem-170	26	6	chemicals	chemical	NOUN
eurjchem-170	26	7	were	be	AUX
eurjchem-170	26	8	also	also	ADV
eurjchem-170	26	9	of	of	ADP
eurjchem-170	26	10	ar	ar	NOUN
eurjchem-170	26	11	grade	grade	NOUN
eurjchem-170	26	12	and	and	CCONJ
eurjchem-170	26	13	bought	buy	VERB
eurjchem-170	26	14	from	from	ADP
eurjchem-170	26	15	local	local	ADJ
eurjchem-170	26	16	suppliers	supplier	NOUN
eurjchem-170	26	17	.	.	PUNCT
eurjchem-170	27	1	hplc	hplc	NOUN
eurjchem-170	27	2	grade	grade	NOUN
eurjchem-170	27	3	acetonitrile	acetonitrile	NOUN
eurjchem-170	27	4	(	(	PUNCT
eurjchem-170	27	5	acn	acn	PROPN
eurjchem-170	27	6	)	)	PUNCT
eurjchem-170	27	7	and	and	CCONJ
eurjchem-170	27	8	methanol	methanol	NOUN
eurjchem-170	27	9	(	(	PUNCT
eurjchem-170	27	10	meoh	meoh	PROPN
eurjchem-170	27	11	)	)	PUNCT
eurjchem-170	27	12	were	be	AUX
eurjchem-170	27	13	procured	procure	VERB
eurjchem-170	27	14	from	from	ADP
eurjchem-170	27	15	j.	j.	PROPN
eurjchem-170	27	16	t.	t.	PROPN
eurjchem-170	27	17	baker	baker	PROPN
eurjchem-170	27	18	(	(	PUNCT
eurjchem-170	27	19	phillipsburg	phillipsburg	PROPN
eurjchem-170	27	20	,	,	PUNCT
eurjchem-170	27	21	nj	nj	PROPN
eurjchem-170	27	22	,	,	PUNCT
eurjchem-170	27	23	usa	usa	PROPN
eurjchem-170	27	24	)	)	PUNCT
eurjchem-170	27	25	.	.	PUNCT
eurjchem-170	28	1	nmr	nmr	NOUN
eurjchem-170	28	2	grade	grade	PROPN
eurjchem-170	28	3	acn	acn	PROPN
eurjchem-170	28	4	and	and	CCONJ
eurjchem-170	28	5	deuterated	deuterate	VERB
eurjchem-170	28	6	water	water	NOUN
eurjchem-170	28	7	(	(	PUNCT
eurjchem-170	28	8	d2o	d2o	NOUN
eurjchem-170	28	9	)	)	PUNCT
eurjchem-170	28	10	of	of	ADP
eurjchem-170	28	11	99.9	99.9	NUM
eurjchem-170	28	12	%	%	NOUN
eurjchem-170	28	13	purity	purity	NOUN
eurjchem-170	28	14	were	be	AUX
eurjchem-170	28	15	obtained	obtain	VERB
eurjchem-170	28	16	from	from	ADP
eurjchem-170	28	17	riedel‐de	riedel‐de	PROPN
eurjchem-170	28	18	haen	haen	PROPN
eurjchem-170	28	19	(	(	PUNCT
eurjchem-170	28	20	seelze	seelze	PROPN
eurjchem-170	28	21	,	,	PUNCT
eurjchem-170	28	22	germany	germany	PROPN
eurjchem-170	28	23	)	)	PUNCT
eurjchem-170	28	24	and	and	CCONJ
eurjchem-170	28	25	aldrich	aldrich	PROPN
eurjchem-170	28	26	(	(	PUNCT
eurjchem-170	28	27	california	california	PROPN
eurjchem-170	28	28	,	,	PUNCT
eurjchem-170	28	29	missouri	missouri	PROPN
eurjchem-170	28	30	,	,	PUNCT
eurjchem-170	28	31	usa	usa	PROPN
eurjchem-170	28	32	)	)	PUNCT
eurjchem-170	28	33	,	,	PUNCT
eurjchem-170	28	34	respectively	respectively	ADV
eurjchem-170	28	35	.	.	PUNCT
eurjchem-170	29	1	es	es	X
eurjchem-170	29	2	tuning	tune	VERB
eurjchem-170	29	3	mix	mix	NOUN
eurjchem-170	29	4	solution	solution	NOUN
eurjchem-170	29	5	(	(	PUNCT
eurjchem-170	29	6	agilent	agilent	PROPN
eurjchem-170	29	7	technologies	technologies	PROPN
eurjchem-170	29	8	,	,	PUNCT
eurjchem-170	29	9	usa	usa	PROPN
eurjchem-170	29	10	)	)	PUNCT
eurjchem-170	29	11	was	be	AUX
eurjchem-170	29	12	used	use	VERB
eurjchem-170	29	13	as	as	ADP
eurjchem-170	29	14	the	the	DET
eurjchem-170	29	15	ms	ms	PROPN
eurjchem-170	29	16	/	/	SYM
eurjchem-170	29	17	tof	tof	PROPN
eurjchem-170	29	18	calibrant	calibrant	NOUN
eurjchem-170	29	19	.	.	PUNCT
eurjchem-170	30	1	water	water	NOUN
eurjchem-170	30	2	for	for	ADP
eurjchem-170	30	3	hplc	hplc	NOUN
eurjchem-170	30	4	studies	study	NOUN
eurjchem-170	30	5	was	be	AUX
eurjchem-170	30	6	obtained	obtain	VERB
eurjchem-170	30	7	from	from	ADP
eurjchem-170	30	8	ultrapure	ultrapure	ADJ
eurjchem-170	30	9	water	water	NOUN
eurjchem-170	30	10	purification	purification	NOUN
eurjchem-170	30	11	unit	unit	NOUN
eurjchem-170	30	12	(	(	PUNCT
eurjchem-170	30	13	elga	elga	PROPN
eurjchem-170	30	14	,	,	PUNCT
eurjchem-170	30	15	wycombe	wycombe	PROPN
eurjchem-170	30	16	,	,	PUNCT
eurjchem-170	30	17	england	england	PROPN
eurjchem-170	30	18	)	)	PUNCT
eurjchem-170	30	19	.	.	PUNCT
eurjchem-170	31	1	2.2	2.2	NUM
eurjchem-170	31	2	.	.	PUNCT
eurjchem-170	31	3	apparatus	apparatus	NOUN
eurjchem-170	31	4	and	and	CCONJ
eurjchem-170	31	5	equipment	equipment	NOUN
eurjchem-170	31	6	precision	precision	NOUN
eurjchem-170	31	7	water	water	NOUN
eurjchem-170	31	8	baths	bath	NOUN
eurjchem-170	31	9	(	(	PUNCT
eurjchem-170	31	10	julabo	julabo	PROPN
eurjchem-170	31	11	,	,	PUNCT
eurjchem-170	31	12	seelbach	seelbach	PROPN
eurjchem-170	31	13	,	,	PUNCT
eurjchem-170	31	14	germany	germany	PROPN
eurjchem-170	31	15	)	)	PUNCT
eurjchem-170	31	16	were	be	AUX
eurjchem-170	31	17	used	use	VERB
eurjchem-170	31	18	for	for	ADP
eurjchem-170	31	19	hydrolytic	hydrolytic	ADJ
eurjchem-170	31	20	studies	study	NOUN
eurjchem-170	31	21	.	.	PUNCT
eurjchem-170	32	1	thermal	thermal	ADJ
eurjchem-170	32	2	stress	stress	NOUN
eurjchem-170	32	3	testing	testing	NOUN
eurjchem-170	32	4	was	be	AUX
eurjchem-170	32	5	carried	carry	VERB
eurjchem-170	32	6	out	out	ADP
eurjchem-170	32	7	using	use	VERB
eurjchem-170	32	8	a	a	DET
eurjchem-170	32	9	dri	dri	PROPN
eurjchem-170	32	10	bath	bath	NOUN
eurjchem-170	32	11	(	(	PUNCT
eurjchem-170	32	12	(	(	PUNCT
eurjchem-170	32	13	thermolyne	thermolyne	PROPN
eurjchem-170	32	14	,	,	PUNCT
eurjchem-170	32	15	iowa	iowa	PROPN
eurjchem-170	32	16	,	,	PUNCT
eurjchem-170	32	17	usa	usa	PROPN
eurjchem-170	32	18	)	)	PUNCT
eurjchem-170	32	19	.	.	PUNCT
eurjchem-170	33	1	the	the	DET
eurjchem-170	33	2	photostability	photostability	PROPN
eurjchem-170	33	3	chamber	chamber	PROPN
eurjchem-170	33	4	(	(	PUNCT
eurjchem-170	33	5	kbwf	kbwf	NOUN
eurjchem-170	33	6	240	240	NUM
eurjchem-170	33	7	,	,	PUNCT
eurjchem-170	33	8	wtc	wtc	PROPN
eurjchem-170	33	9	binder	binder	PROPN
eurjchem-170	33	10	,	,	PUNCT
eurjchem-170	33	11	tuttlingen	tuttlingen	PROPN
eurjchem-170	33	12	,	,	PUNCT
eurjchem-170	33	13	germany	germany	PROPN
eurjchem-170	33	14	)	)	PUNCT
eurjchem-170	33	15	was	be	AUX
eurjchem-170	33	16	equipped	equip	VERB
eurjchem-170	33	17	with	with	ADP
eurjchem-170	33	18	an	an	DET
eurjchem-170	33	19	illumination	illumination	NOUN
eurjchem-170	33	20	bank	bank	NOUN
eurjchem-170	33	21	on	on	ADP
eurjchem-170	33	22	the	the	DET
eurjchem-170	33	23	inside	inside	ADJ
eurjchem-170	33	24	top	top	NOUN
eurjchem-170	33	25	,	,	PUNCT
eurjchem-170	33	26	consisting	consist	VERB
eurjchem-170	33	27	of	of	ADP
eurjchem-170	33	28	a	a	DET
eurjchem-170	33	29	combination	combination	NOUN
eurjchem-170	33	30	of	of	ADP
eurjchem-170	33	31	two	two	NUM
eurjchem-170	33	32	uv	uv	NOUN
eurjchem-170	33	33	(	(	PUNCT
eurjchem-170	33	34	osram	osram	PROPN
eurjchem-170	33	35	l18	l18	PROPN
eurjchem-170	33	36	w/73	w/73	PROPN
eurjchem-170	33	37	)	)	PUNCT
eurjchem-170	33	38	and	and	CCONJ
eurjchem-170	33	39	four	four	NUM
eurjchem-170	33	40	white	white	ADJ
eurjchem-170	33	41	fluorescent	fluorescent	NOUN
eurjchem-170	33	42	(	(	PUNCT
eurjchem-170	33	43	philips	philips	PROPN
eurjchem-170	33	44	trulite	trulite	PROPN
eurjchem-170	33	45	18w/86	18w/86	NUM
eurjchem-170	33	46	)	)	PUNCT
eurjchem-170	33	47	lamps	lamp	NOUN
eurjchem-170	33	48	,	,	PUNCT
eurjchem-170	33	49	in	in	ADP
eurjchem-170	33	50	accordance	accordance	NOUN
eurjchem-170	33	51	with	with	ADP
eurjchem-170	33	52	option	option	NOUN
eurjchem-170	33	53	2	2	NUM
eurjchem-170	33	54	of	of	ADP
eurjchem-170	33	55	the	the	DET
eurjchem-170	33	56	ich	ich	NOUN
eurjchem-170	33	57	guideline	guideline	NOUN
eurjchem-170	33	58	q1b	q1b	PROPN
eurjchem-170	33	59	[	[	X
eurjchem-170	33	60	14	14	NUM
eurjchem-170	33	61	]	]	PUNCT
eurjchem-170	33	62	.	.	PUNCT
eurjchem-170	34	1	both	both	PRON
eurjchem-170	34	2	fluorescent	fluorescent	ADJ
eurjchem-170	34	3	and	and	CCONJ
eurjchem-170	34	4	uv	uv	NOUN
eurjchem-170	34	5	lamps	lamp	NOUN
eurjchem-170	34	6	were	be	AUX
eurjchem-170	34	7	put	put	VERB
eurjchem-170	34	8	on	on	ADP
eurjchem-170	34	9	simultaneously	simultaneously	ADV
eurjchem-170	34	10	.	.	PUNCT
eurjchem-170	35	1	the	the	DET
eurjchem-170	35	2	samples	sample	NOUN
eurjchem-170	35	3	were	be	AUX
eurjchem-170	35	4	placed	place	VERB
eurjchem-170	35	5	at	at	ADP
eurjchem-170	35	6	a	a	DET
eurjchem-170	35	7	distance	distance	NOUN
eurjchem-170	35	8	of	of	ADP
eurjchem-170	35	9	9	9	NUM
eurjchem-170	35	10	inches	inch	NOUN
eurjchem-170	35	11	from	from	ADP
eurjchem-170	35	12	the	the	DET
eurjchem-170	35	13	light	light	ADJ
eurjchem-170	35	14	bank	bank	NOUN
eurjchem-170	35	15	.	.	PUNCT
eurjchem-170	36	1	a	a	DET
eurjchem-170	36	2	lux	lux	NOUN
eurjchem-170	36	3	meter	meter	NOUN
eurjchem-170	36	4	(	(	PUNCT
eurjchem-170	36	5	model	model	NOUN
eurjchem-170	36	6	elm	elm	PROPN
eurjchem-170	36	7	201	201	NUM
eurjchem-170	36	8	,	,	PUNCT
eurjchem-170	36	9	escorp	escorp	PROPN
eurjchem-170	36	10	,	,	PUNCT
eurjchem-170	36	11	new	new	ADJ
eurjchem-170	36	12	delhi	delhi	PROPN
eurjchem-170	36	13	,	,	PUNCT
eurjchem-170	36	14	india	india	PROPN
eurjchem-170	36	15	)	)	PUNCT
eurjchem-170	36	16	and	and	CCONJ
eurjchem-170	36	17	a	a	DET
eurjchem-170	36	18	uv	uv	NOUN
eurjchem-170	36	19	radiometer	radiometer	NOUN
eurjchem-170	36	20	(	(	PUNCT
eurjchem-170	36	21	model	model	NOUN
eurjchem-170	36	22	206	206	NUM
eurjchem-170	36	23	,	,	PUNCT
eurjchem-170	36	24	prc	prc	PROPN
eurjchem-170	36	25	krochmann	krochmann	PROPN
eurjchem-170	36	26	gmbh	gmbh	PROPN
eurjchem-170	36	27	,	,	PUNCT
eurjchem-170	36	28	berlin	berlin	PROPN
eurjchem-170	36	29	,	,	PUNCT
eurjchem-170	36	30	germany	germany	PROPN
eurjchem-170	36	31	)	)	PUNCT
eurjchem-170	36	32	were	be	AUX
eurjchem-170	36	33	used	use	VERB
eurjchem-170	36	34	to	to	PART
eurjchem-170	36	35	measure	measure	VERB
eurjchem-170	36	36	visible	visible	ADJ
eurjchem-170	36	37	illumination	illumination	NOUN
eurjchem-170	36	38	and	and	CCONJ
eurjchem-170	36	39	uv	uv	NOUN
eurjchem-170	36	40	energy	energy	NOUN
eurjchem-170	36	41	,	,	PUNCT
eurjchem-170	36	42	respectively	respectively	ADV
eurjchem-170	36	43	.	.	PUNCT
eurjchem-170	37	1	other	other	ADJ
eurjchem-170	37	2	equipments	equipment	NOUN
eurjchem-170	37	3	used	use	VERB
eurjchem-170	37	4	for	for	ADP
eurjchem-170	37	5	the	the	DET
eurjchem-170	37	6	study	study	NOUN
eurjchem-170	37	7	were	be	AUX
eurjchem-170	37	8	sonicator	sonicator	NOUN
eurjchem-170	37	9	(	(	PUNCT
eurjchem-170	37	10	3210	3210	NUM
eurjchem-170	37	11	,	,	PUNCT
eurjchem-170	37	12	branson	branson	PROPN
eurjchem-170	37	13	shah	shah	PROPN
eurjchem-170	37	14	et	et	PROPN
eurjchem-170	37	15	al	al	PROPN
eurjchem-170	37	16	.	.	PUNCT
eurjchem-170	37	17	/	/	SYM
eurjchem-170	37	18	european	european	PROPN
eurjchem-170	37	19	journal	journal	PROPN
eurjchem-170	37	20	of	of	ADP
eurjchem-170	37	21	chemistry	chemistry	NOUN
eurjchem-170	37	22	2	2	NUM
eurjchem-170	37	23	(	(	PUNCT
eurjchem-170	37	24	2	2	NUM
eurjchem-170	37	25	)	)	PUNCT
eurjchem-170	37	26	(	(	PUNCT
eurjchem-170	37	27	2011	2011	NUM
eurjchem-170	37	28	)	)	PUNCT
eurjchem-170	38	1	152‐157	152‐157	NOUN
eurjchem-170	38	2	153	153	NUM
eurjchem-170	38	3	ultrasoincs	ultrasoinc	NOUN
eurjchem-170	38	4	corporation	corporation	NOUN
eurjchem-170	38	5	,	,	PUNCT
eurjchem-170	38	6	ct	ct	PROPN
eurjchem-170	38	7	,	,	PUNCT
eurjchem-170	38	8	usa	usa	PROPN
eurjchem-170	38	9	)	)	PUNCT
eurjchem-170	38	10	,	,	PUNCT
eurjchem-170	38	11	precision	precision	NOUN
eurjchem-170	38	12	analytical	analytical	ADJ
eurjchem-170	38	13	balance	balance	NOUN
eurjchem-170	38	14	(	(	PUNCT
eurjchem-170	38	15	ag	ag	PROPN
eurjchem-170	38	16	135	135	NUM
eurjchem-170	38	17	,	,	PUNCT
eurjchem-170	38	18	mettler	mettler	PROPN
eurjchem-170	38	19	toledo	toledo	PROPN
eurjchem-170	38	20	,	,	PUNCT
eurjchem-170	38	21	schwerzenbach	schwerzenbach	NOUN
eurjchem-170	38	22	,	,	PUNCT
eurjchem-170	38	23	switzerland	switzerland	PROPN
eurjchem-170	38	24	)	)	PUNCT
eurjchem-170	38	25	,	,	PUNCT
eurjchem-170	38	26	ph	ph	ADJ
eurjchem-170	38	27	/	/	SYM
eurjchem-170	38	28	ion	ion	NOUN
eurjchem-170	38	29	analyzer	analyzer	NOUN
eurjchem-170	38	30	(	(	PUNCT
eurjchem-170	38	31	ma	ma	PROPN
eurjchem-170	38	32	235	235	NUM
eurjchem-170	38	33	,	,	PUNCT
eurjchem-170	38	34	mettler	mettler	PROPN
eurjchem-170	38	35	toledo	toledo	PROPN
eurjchem-170	38	36	,	,	PUNCT
eurjchem-170	38	37	schwerzenbach	schwerzenbach	NOUN
eurjchem-170	38	38	,	,	PUNCT
eurjchem-170	38	39	switzerland	switzerland	PROPN
eurjchem-170	38	40	)	)	PUNCT
eurjchem-170	38	41	and	and	CCONJ
eurjchem-170	38	42	autopipettes	autopipette	NOUN
eurjchem-170	38	43	(	(	PUNCT
eurjchem-170	38	44	eppendorf	eppendorf	PROPN
eurjchem-170	38	45	,	,	PUNCT
eurjchem-170	38	46	hamburg	hamburg	PROPN
eurjchem-170	38	47	,	,	PUNCT
eurjchem-170	38	48	germany	germany	PROPN
eurjchem-170	38	49	)	)	PUNCT
eurjchem-170	38	50	.	.	PUNCT
eurjchem-170	39	1	the	the	DET
eurjchem-170	39	2	stand‐alone	stand‐alone	PROPN
eurjchem-170	39	3	hplc	hplc	NOUN
eurjchem-170	39	4	system	system	NOUN
eurjchem-170	39	5	was	be	AUX
eurjchem-170	39	6	vp	vp	PROPN
eurjchem-170	39	7	series	series	NOUN
eurjchem-170	39	8	from	from	ADP
eurjchem-170	39	9	shimadzu	shimadzu	PROPN
eurjchem-170	39	10	(	(	PUNCT
eurjchem-170	39	11	kyoto	kyoto	PROPN
eurjchem-170	39	12	,	,	PUNCT
eurjchem-170	39	13	japan	japan	PROPN
eurjchem-170	39	14	)	)	PUNCT
eurjchem-170	39	15	and	and	CCONJ
eurjchem-170	39	16	was	be	AUX
eurjchem-170	39	17	equipped	equip	VERB
eurjchem-170	39	18	with	with	ADP
eurjchem-170	39	19	a	a	DET
eurjchem-170	39	20	photodiode	photodiode	NOUN
eurjchem-170	39	21	array	array	NOUN
eurjchem-170	39	22	detector	detector	NOUN
eurjchem-170	39	23	.	.	PUNCT
eurjchem-170	40	1	it	it	PRON
eurjchem-170	40	2	was	be	AUX
eurjchem-170	40	3	controlled	control	VERB
eurjchem-170	40	4	by	by	ADP
eurjchem-170	40	5	sp1	sp1	PROPN
eurjchem-170	40	6	software	software	NOUN
eurjchem-170	40	7	ver	ver	NOUN
eurjchem-170	40	8	.	.	PUNCT
eurjchem-170	41	1	6.14	6.14	NUM
eurjchem-170	41	2	.	.	PUNCT
eurjchem-170	42	1	lc‐	lc‐	ADJ
eurjchem-170	42	2	ms	ms	PROPN
eurjchem-170	42	3	/	/	SYM
eurjchem-170	42	4	tof	tof	PROPN
eurjchem-170	42	5	results	result	NOUN
eurjchem-170	42	6	were	be	AUX
eurjchem-170	42	7	obtained	obtain	VERB
eurjchem-170	42	8	on	on	ADP
eurjchem-170	42	9	a	a	DET
eurjchem-170	42	10	system	system	NOUN
eurjchem-170	42	11	in	in	ADP
eurjchem-170	42	12	which	which	PRON
eurjchem-170	42	13	lc	lc	PROPN
eurjchem-170	42	14	(	(	PUNCT
eurjchem-170	42	15	model	model	NOUN
eurjchem-170	42	16	1100	1100	NUM
eurjchem-170	42	17	,	,	PUNCT
eurjchem-170	42	18	agilent	agilent	PROPN
eurjchem-170	42	19	technologies	technology	NOUN
eurjchem-170	42	20	,	,	PUNCT
eurjchem-170	42	21	waldbronn	waldbronn	NOUN
eurjchem-170	42	22	,	,	PUNCT
eurjchem-170	42	23	germany	germany	PROPN
eurjchem-170	42	24	)	)	PUNCT
eurjchem-170	42	25	was	be	AUX
eurjchem-170	42	26	hyphenated	hyphenate	VERB
eurjchem-170	42	27	to	to	ADP
eurjchem-170	42	28	microtof‐q	microtof‐q	NOUN
eurjchem-170	42	29	spectrometer	spectrometer	NOUN
eurjchem-170	42	30	(	(	PUNCT
eurjchem-170	42	31	bruker	bruker	PROPN
eurjchem-170	42	32	daltonik	daltonik	NOUN
eurjchem-170	42	33	,	,	PUNCT
eurjchem-170	42	34	bremen	bremen	PROPN
eurjchem-170	42	35	,	,	PUNCT
eurjchem-170	42	36	germany	germany	PROPN
eurjchem-170	42	37	)	)	PUNCT
eurjchem-170	42	38	using	use	VERB
eurjchem-170	42	39	hyphenation	hyphenation	PROPN
eurjchem-170	42	40	star	star	NOUN
eurjchem-170	42	41	(	(	PUNCT
eurjchem-170	42	42	version	version	NOUN
eurjchem-170	42	43	3.1	3.1	NUM
eurjchem-170	42	44	)	)	PUNCT
eurjchem-170	42	45	and	and	CCONJ
eurjchem-170	42	46	microtof	microtof	NOUN
eurjchem-170	42	47	control	control	PROPN
eurjchem-170	42	48	(	(	PUNCT
eurjchem-170	42	49	version	version	NOUN
eurjchem-170	42	50	2.0	2.0	NUM
eurjchem-170	42	51	)	)	PUNCT
eurjchem-170	42	52	software	software	NOUN
eurjchem-170	42	53	.	.	PUNCT
eurjchem-170	43	1	multi‐stage	multi‐stage	NOUN
eurjchem-170	43	2	mass	mass	NOUN
eurjchem-170	43	3	(	(	PUNCT
eurjchem-170	43	4	msn	msn	NOUN
eurjchem-170	43	5	)	)	PUNCT
eurjchem-170	43	6	studies	study	NOUN
eurjchem-170	43	7	were	be	AUX
eurjchem-170	43	8	carried	carry	VERB
eurjchem-170	43	9	out	out	ADP
eurjchem-170	43	10	on	on	ADP
eurjchem-170	43	11	a	a	DET
eurjchem-170	43	12	ltq	ltq	NOUN
eurjchem-170	43	13	xl	xl	PROPN
eurjchem-170	43	14	ms	ms	PROPN
eurjchem-170	43	15	2.5.0	2.5.0	NUM
eurjchem-170	43	16	system	system	NOUN
eurjchem-170	43	17	(	(	PUNCT
eurjchem-170	43	18	thermo	thermo	NOUN
eurjchem-170	43	19	,	,	PUNCT
eurjchem-170	43	20	san	san	PROPN
eurjchem-170	43	21	jose	jose	PROPN
eurjchem-170	43	22	,	,	PUNCT
eurjchem-170	43	23	usa	usa	PROPN
eurjchem-170	43	24	)	)	PUNCT
eurjchem-170	43	25	.	.	PUNCT
eurjchem-170	44	1	the	the	DET
eurjchem-170	44	2	same	same	ADJ
eurjchem-170	44	3	was	be	AUX
eurjchem-170	44	4	controlled	control	VERB
eurjchem-170	44	5	by	by	ADP
eurjchem-170	44	6	xcalibur	xcalibur	PROPN
eurjchem-170	44	7	(	(	PUNCT
eurjchem-170	44	8	version	version	NOUN
eurjchem-170	44	9	2.0.7	2.0.7	NUM
eurjchem-170	44	10	sp1	sp1	NOUN
eurjchem-170	44	11	)	)	PUNCT
eurjchem-170	44	12	software	software	NOUN
eurjchem-170	44	13	.	.	PUNCT
eurjchem-170	45	1	the	the	DET
eurjchem-170	45	2	microtof‐q	microtof‐q	PROPN
eurjchem-170	45	3	instrument	instrument	NOUN
eurjchem-170	45	4	was	be	AUX
eurjchem-170	45	5	also	also	ADV
eurjchem-170	45	6	used	use	VERB
eurjchem-170	45	7	for	for	ADP
eurjchem-170	45	8	h	h	NOUN
eurjchem-170	45	9	/	/	SYM
eurjchem-170	45	10	d	d	PROPN
eurjchem-170	45	11	exchange	exchange	NOUN
eurjchem-170	45	12	study	study	NOUN
eurjchem-170	45	13	on	on	ADP
eurjchem-170	45	14	the	the	DET
eurjchem-170	45	15	drug	drug	NOUN
eurjchem-170	45	16	,	,	PUNCT
eurjchem-170	45	17	while	while	SCONJ
eurjchem-170	45	18	ltq	ltq	PROPN
eurjchem-170	45	19	xl	xl	PROPN
eurjchem-170	45	20	system	system	NOUN
eurjchem-170	45	21	was	be	AUX
eurjchem-170	45	22	employed	employ	VERB
eurjchem-170	45	23	for	for	ADP
eurjchem-170	45	24	on‐line	on‐line	NOUN
eurjchem-170	45	25	h	h	NOUN
eurjchem-170	45	26	/	/	SYM
eurjchem-170	45	27	d	d	NOUN
eurjchem-170	45	28	exchange	exchange	NOUN
eurjchem-170	45	29	investigations	investigation	NOUN
eurjchem-170	45	30	on	on	ADP
eurjchem-170	45	31	the	the	DET
eurjchem-170	45	32	product	product	NOUN
eurjchem-170	45	33	.	.	PUNCT
eurjchem-170	46	1	lc‐nmr	lc‐nmr	ADJ
eurjchem-170	46	2	measurements	measurement	NOUN
eurjchem-170	46	3	were	be	AUX
eurjchem-170	46	4	done	do	VERB
eurjchem-170	46	5	using	use	VERB
eurjchem-170	46	6	jnm‐	jnm‐	PROPN
eurjchem-170	46	7	eca	eca	NOUN
eurjchem-170	46	8	500	500	NUM
eurjchem-170	46	9	mhz	mhz	NOUN
eurjchem-170	46	10	spectrometer	spectrometer	NOUN
eurjchem-170	46	11	(	(	PUNCT
eurjchem-170	46	12	jeol	jeol	PROPN
eurjchem-170	46	13	,	,	PUNCT
eurjchem-170	46	14	tokyo	tokyo	PROPN
eurjchem-170	46	15	,	,	PUNCT
eurjchem-170	46	16	japan	japan	PROPN
eurjchem-170	46	17	)	)	PUNCT
eurjchem-170	46	18	coupled	couple	VERB
eurjchem-170	46	19	to	to	ADP
eurjchem-170	46	20	prominence	prominence	NOUN
eurjchem-170	46	21	lc	lc	NOUN
eurjchem-170	46	22	system	system	NOUN
eurjchem-170	46	23	(	(	PUNCT
eurjchem-170	46	24	shimadzu	shimadzu	PROPN
eurjchem-170	46	25	,	,	PUNCT
eurjchem-170	46	26	kyoto	kyoto	PROPN
eurjchem-170	46	27	,	,	PUNCT
eurjchem-170	46	28	japan	japan	PROPN
eurjchem-170	46	29	)	)	PUNCT
eurjchem-170	46	30	and	and	CCONJ
eurjchem-170	46	31	controlled	control	VERB
eurjchem-170	46	32	by	by	ADP
eurjchem-170	46	33	delta	delta	PROPN
eurjchem-170	46	34	(	(	PUNCT
eurjchem-170	46	35	version	version	NOUN
eurjchem-170	46	36	4.3	4.3	NUM
eurjchem-170	46	37	)	)	PUNCT
eurjchem-170	46	38	and	and	CCONJ
eurjchem-170	46	39	lc‐nmr	lc‐nmr	ADJ
eurjchem-170	46	40	dio	dio	NOUN
eurjchem-170	46	41	(	(	PUNCT
eurjchem-170	46	42	version	version	NOUN
eurjchem-170	46	43	2.0	2.0	NUM
eurjchem-170	46	44	)	)	PUNCT
eurjchem-170	46	45	software	software	NOUN
eurjchem-170	46	46	,	,	PUNCT
eurjchem-170	46	47	respectively	respectively	ADV
eurjchem-170	46	48	.	.	PUNCT
eurjchem-170	47	1	2.3	2.3	NUM
eurjchem-170	47	2	.	.	PUNCT
eurjchem-170	47	3	stress	stress	NOUN
eurjchem-170	47	4	testing	test	VERB
eurjchem-170	47	5	the	the	DET
eurjchem-170	47	6	stressors	stressor	NOUN
eurjchem-170	47	7	,	,	PUNCT
eurjchem-170	47	8	choice	choice	NOUN
eurjchem-170	47	9	of	of	ADP
eurjchem-170	47	10	their	their	PRON
eurjchem-170	47	11	concentration	concentration	NOUN
eurjchem-170	47	12	and	and	CCONJ
eurjchem-170	47	13	preparation	preparation	NOUN
eurjchem-170	47	14	of	of	ADP
eurjchem-170	47	15	samples	sample	NOUN
eurjchem-170	47	16	were	be	AUX
eurjchem-170	47	17	based	base	VERB
eurjchem-170	47	18	on	on	ADP
eurjchem-170	47	19	our	our	PRON
eurjchem-170	47	20	previous	previous	ADJ
eurjchem-170	47	21	publication	publication	NOUN
eurjchem-170	47	22	[	[	X
eurjchem-170	47	23	15	15	NUM
eurjchem-170	47	24	]	]	PUNCT
eurjchem-170	47	25	.	.	PUNCT
eurjchem-170	48	1	as	as	SCONJ
eurjchem-170	48	2	the	the	DET
eurjchem-170	48	3	drug	drug	NOUN
eurjchem-170	48	4	was	be	AUX
eurjchem-170	48	5	insoluble	insoluble	ADJ
eurjchem-170	48	6	in	in	ADP
eurjchem-170	48	7	water	water	NOUN
eurjchem-170	48	8	,	,	PUNCT
eurjchem-170	48	9	it	it	PRON
eurjchem-170	48	10	was	be	AUX
eurjchem-170	48	11	dissolved	dissolve	VERB
eurjchem-170	48	12	in	in	ADP
eurjchem-170	48	13	a	a	DET
eurjchem-170	48	14	mixture	mixture	NOUN
eurjchem-170	48	15	of	of	ADP
eurjchem-170	48	16	acn	acn	PROPN
eurjchem-170	48	17	and	and	CCONJ
eurjchem-170	48	18	water	water	NOUN
eurjchem-170	48	19	in	in	ADP
eurjchem-170	48	20	a	a	DET
eurjchem-170	48	21	ratio	ratio	NOUN
eurjchem-170	48	22	of	of	ADP
eurjchem-170	48	23	50:50	50:50	NUM
eurjchem-170	48	24	(	(	PUNCT
eurjchem-170	48	25	v	v	NOUN
eurjchem-170	48	26	:	:	PUNCT
eurjchem-170	48	27	v	v	NOUN
eurjchem-170	48	28	)	)	PUNCT
eurjchem-170	48	29	to	to	PART
eurjchem-170	48	30	achieve	achieve	VERB
eurjchem-170	48	31	a	a	DET
eurjchem-170	48	32	stock	stock	NOUN
eurjchem-170	48	33	concentration	concentration	NOUN
eurjchem-170	48	34	of	of	ADP
eurjchem-170	48	35	2	2	NUM
eurjchem-170	48	36	mg	mg	NUM
eurjchem-170	48	37	/	/	SYM
eurjchem-170	48	38	ml	ml	NOUN
eurjchem-170	48	39	.	.	PUNCT
eurjchem-170	49	1	this	this	DET
eurjchem-170	49	2	stock	stock	NOUN
eurjchem-170	49	3	was	be	AUX
eurjchem-170	49	4	diluted	dilute	VERB
eurjchem-170	49	5	50:50	50:50	NUM
eurjchem-170	49	6	(	(	PUNCT
eurjchem-170	49	7	v	v	NOUN
eurjchem-170	49	8	:	:	PUNCT
eurjchem-170	49	9	v	v	NOUN
eurjchem-170	49	10	)	)	PUNCT
eurjchem-170	49	11	with	with	ADP
eurjchem-170	49	12	the	the	DET
eurjchem-170	49	13	stressor	stressor	NOUN
eurjchem-170	49	14	(	(	PUNCT
eurjchem-170	49	15	e.g.	e.g.	ADV
eurjchem-170	49	16	,	,	PUNCT
eurjchem-170	49	17	hcl	hcl	PROPN
eurjchem-170	49	18	,	,	PUNCT
eurjchem-170	49	19	water	water	NOUN
eurjchem-170	49	20	,	,	PUNCT
eurjchem-170	49	21	naoh	naoh	NOUN
eurjchem-170	49	22	or	or	CCONJ
eurjchem-170	49	23	h2o2	h2o2	NOUN
eurjchem-170	49	24	)	)	PUNCT
eurjchem-170	49	25	.	.	PUNCT
eurjchem-170	50	1	hydrolytic	hydrolytic	ADJ
eurjchem-170	50	2	decomposition	decomposition	NOUN
eurjchem-170	50	3	of	of	ADP
eurjchem-170	50	4	the	the	DET
eurjchem-170	50	5	drug	drug	NOUN
eurjchem-170	50	6	was	be	AUX
eurjchem-170	50	7	carried	carry	VERB
eurjchem-170	50	8	out	out	ADP
eurjchem-170	50	9	in	in	ADP
eurjchem-170	50	10	1	1	NUM
eurjchem-170	50	11	n	n	PRON
eurjchem-170	50	12	hcl	hcl	NOUN
eurjchem-170	50	13	,	,	PUNCT
eurjchem-170	50	14	water	water	NOUN
eurjchem-170	50	15	and	and	CCONJ
eurjchem-170	50	16	1	1	NUM
eurjchem-170	50	17	n	n	NOUN
eurjchem-170	50	18	naoh	naoh	NOUN
eurjchem-170	50	19	at	at	ADP
eurjchem-170	50	20	80	80	NUM
eurjchem-170	50	21	°	°	NUM
eurjchem-170	50	22	c	c	NOUN
eurjchem-170	50	23	for	for	ADP
eurjchem-170	50	24	48	48	NUM
eurjchem-170	50	25	h.	h.	NOUN
eurjchem-170	50	26	the	the	DET
eurjchem-170	50	27	oxidative	oxidative	ADJ
eurjchem-170	50	28	study	study	NOUN
eurjchem-170	50	29	was	be	AUX
eurjchem-170	50	30	carried	carry	VERB
eurjchem-170	50	31	out	out	ADP
eurjchem-170	50	32	in	in	ADP
eurjchem-170	50	33	15	15	NUM
eurjchem-170	50	34	%	%	NOUN
eurjchem-170	50	35	v	v	ADP
eurjchem-170	50	36	/	/	SYM
eurjchem-170	50	37	v	v	NOUN
eurjchem-170	50	38	h2o2	h2o2	NOUN
eurjchem-170	50	39	at	at	ADP
eurjchem-170	50	40	room	room	NOUN
eurjchem-170	50	41	temperature	temperature	NOUN
eurjchem-170	50	42	for	for	ADP
eurjchem-170	50	43	2	2	NUM
eurjchem-170	50	44	d.	d.	PROPN
eurjchem-170	50	45	photolytic	photolytic	PROPN
eurjchem-170	50	46	studies	study	NOUN
eurjchem-170	50	47	on	on	ADP
eurjchem-170	50	48	the	the	DET
eurjchem-170	50	49	drug	drug	NOUN
eurjchem-170	50	50	in	in	ADP
eurjchem-170	50	51	the	the	DET
eurjchem-170	50	52	solution	solution	NOUN
eurjchem-170	50	53	state	state	NOUN
eurjchem-170	50	54	were	be	AUX
eurjchem-170	50	55	carried	carry	VERB
eurjchem-170	50	56	out	out	ADP
eurjchem-170	50	57	in	in	ADP
eurjchem-170	50	58	0.1	0.1	NUM
eurjchem-170	50	59	n	n	PRON
eurjchem-170	50	60	hcl	hcl	NOUN
eurjchem-170	50	61	,	,	PUNCT
eurjchem-170	50	62	water	water	NOUN
eurjchem-170	50	63	and	and	CCONJ
eurjchem-170	50	64	0.1	0.1	NUM
eurjchem-170	50	65	n	n	PRON
eurjchem-170	50	66	naoh	naoh	NOUN
eurjchem-170	50	67	by	by	ADP
eurjchem-170	50	68	exposing	expose	VERB
eurjchem-170	50	69	the	the	DET
eurjchem-170	50	70	same	same	ADJ
eurjchem-170	50	71	for	for	ADP
eurjchem-170	50	72	13	13	NUM
eurjchem-170	50	73	,	,	PUNCT
eurjchem-170	50	74	13	13	NUM
eurjchem-170	50	75	and	and	CCONJ
eurjchem-170	50	76	4	4	NUM
eurjchem-170	50	77	d	d	NOUN
eurjchem-170	50	78	,	,	PUNCT
eurjchem-170	50	79	respectively	respectively	ADV
eurjchem-170	50	80	,	,	PUNCT
eurjchem-170	50	81	in	in	ADP
eurjchem-170	50	82	a	a	DET
eurjchem-170	50	83	photostability	photostability	NOUN
eurjchem-170	50	84	chamber	chamber	NOUN
eurjchem-170	50	85	delivering	deliver	VERB
eurjchem-170	50	86	8500	8500	NUM
eurjchem-170	50	87	lx	lx	NOUN
eurjchem-170	50	88	of	of	ADP
eurjchem-170	50	89	fluorescent	fluorescent	NOUN
eurjchem-170	50	90	and	and	CCONJ
eurjchem-170	50	91	0.5	0.5	NUM
eurjchem-170	50	92	w	w	PROPN
eurjchem-170	50	93	/	/	SYM
eurjchem-170	50	94	m2	m2	PROPN
eurjchem-170	50	95	of	of	ADP
eurjchem-170	50	96	uv	uv	NOUN
eurjchem-170	50	97	light	light	NOUN
eurjchem-170	50	98	and	and	CCONJ
eurjchem-170	50	99	set	set	VERB
eurjchem-170	50	100	at	at	ADP
eurjchem-170	50	101	40±1	40±1	PROPN
eurjchem-170	50	102	°	°	PROPN
eurjchem-170	51	1	c/75±3	c/75±3	PROPN
eurjchem-170	51	2	%	%	NOUN
eurjchem-170	51	3	rh	rh	PROPN
eurjchem-170	51	4	.	.	PUNCT
eurjchem-170	51	5	photolytic	photolytic	PROPN
eurjchem-170	51	6	studies	study	NOUN
eurjchem-170	51	7	in	in	ADP
eurjchem-170	51	8	the	the	DET
eurjchem-170	51	9	solid	solid	ADJ
eurjchem-170	51	10	state	state	NOUN
eurjchem-170	51	11	were	be	AUX
eurjchem-170	51	12	performed	perform	VERB
eurjchem-170	51	13	for	for	ADP
eurjchem-170	51	14	13	13	NUM
eurjchem-170	51	15	d	d	NOUN
eurjchem-170	51	16	by	by	ADP
eurjchem-170	51	17	exposing	expose	VERB
eurjchem-170	51	18	a	a	DET
eurjchem-170	51	19	thin	thin	ADJ
eurjchem-170	51	20	layer	layer	NOUN
eurjchem-170	51	21	of	of	ADP
eurjchem-170	51	22	the	the	DET
eurjchem-170	51	23	drug	drug	NOUN
eurjchem-170	51	24	to	to	PART
eurjchem-170	51	25	light	light	VERB
eurjchem-170	51	26	under	under	ADP
eurjchem-170	51	27	the	the	DET
eurjchem-170	51	28	same	same	ADJ
eurjchem-170	51	29	conditions	condition	NOUN
eurjchem-170	51	30	as	as	ADP
eurjchem-170	51	31	in	in	ADP
eurjchem-170	51	32	solution	solution	NOUN
eurjchem-170	51	33	state	state	NOUN
eurjchem-170	51	34	.	.	PUNCT
eurjchem-170	52	1	parallel	parallel	ADJ
eurjchem-170	52	2	blank	blank	ADJ
eurjchem-170	52	3	sets	set	NOUN
eurjchem-170	52	4	were	be	AUX
eurjchem-170	52	5	kept	keep	VERB
eurjchem-170	52	6	in	in	ADP
eurjchem-170	52	7	the	the	DET
eurjchem-170	52	8	dark	dark	NOUN
eurjchem-170	52	9	for	for	ADP
eurjchem-170	52	10	respective	respective	ADJ
eurjchem-170	52	11	time	time	NOUN
eurjchem-170	52	12	points	point	NOUN
eurjchem-170	52	13	.	.	PUNCT
eurjchem-170	53	1	for	for	ADP
eurjchem-170	53	2	thermal	thermal	ADJ
eurjchem-170	53	3	stress	stress	NOUN
eurjchem-170	53	4	testing	testing	NOUN
eurjchem-170	53	5	,	,	PUNCT
eurjchem-170	53	6	the	the	DET
eurjchem-170	53	7	drug	drug	NOUN
eurjchem-170	53	8	was	be	AUX
eurjchem-170	53	9	sealed	seal	VERB
eurjchem-170	53	10	in	in	ADP
eurjchem-170	53	11	glass	glass	NOUN
eurjchem-170	53	12	vials	vial	NOUN
eurjchem-170	53	13	and	and	CCONJ
eurjchem-170	53	14	placed	place	VERB
eurjchem-170	53	15	in	in	ADP
eurjchem-170	53	16	a	a	DET
eurjchem-170	53	17	thermostatic	thermostatic	ADJ
eurjchem-170	53	18	block	block	NOUN
eurjchem-170	53	19	at	at	ADP
eurjchem-170	53	20	50	50	NUM
eurjchem-170	53	21	°	°	NOUN
eurjchem-170	53	22	c	c	NOUN
eurjchem-170	53	23	for	for	ADP
eurjchem-170	53	24	21	21	NUM
eurjchem-170	53	25	d	d	NOUN
eurjchem-170	53	26	to	to	PART
eurjchem-170	53	27	see	see	VERB
eurjchem-170	53	28	the	the	DET
eurjchem-170	53	29	effect	effect	NOUN
eurjchem-170	53	30	of	of	ADP
eurjchem-170	53	31	heat	heat	NOUN
eurjchem-170	53	32	alone	alone	ADV
eurjchem-170	53	33	on	on	ADP
eurjchem-170	53	34	the	the	DET
eurjchem-170	53	35	drug	drug	NOUN
eurjchem-170	53	36	molecule	molecule	NOUN
eurjchem-170	53	37	.	.	PUNCT
eurjchem-170	54	1	after	after	ADP
eurjchem-170	54	2	subjecting	subject	VERB
eurjchem-170	54	3	to	to	ADP
eurjchem-170	54	4	stress	stress	NOUN
eurjchem-170	54	5	,	,	PUNCT
eurjchem-170	54	6	samples	sample	NOUN
eurjchem-170	54	7	were	be	AUX
eurjchem-170	54	8	withdrawn	withdraw	VERB
eurjchem-170	54	9	at	at	ADP
eurjchem-170	54	10	suitable	suitable	ADJ
eurjchem-170	54	11	time	time	NOUN
eurjchem-170	54	12	intervals	interval	NOUN
eurjchem-170	54	13	and	and	CCONJ
eurjchem-170	54	14	diluted	dilute	VERB
eurjchem-170	54	15	four	four	NUM
eurjchem-170	54	16	folds	fold	NOUN
eurjchem-170	54	17	with	with	ADP
eurjchem-170	54	18	acn	acn	PROPN
eurjchem-170	54	19	and	and	CCONJ
eurjchem-170	54	20	water	water	NOUN
eurjchem-170	54	21	(	(	PUNCT
eurjchem-170	54	22	50:50	50:50	NUM
eurjchem-170	54	23	,	,	PUNCT
eurjchem-170	54	24	v	v	NOUN
eurjchem-170	54	25	:	:	PUNCT
eurjchem-170	54	26	v	v	NOUN
eurjchem-170	54	27	)	)	PUNCT
eurjchem-170	54	28	before	before	ADP
eurjchem-170	54	29	injection	injection	NOUN
eurjchem-170	54	30	into	into	ADP
eurjchem-170	54	31	hplc	hplc	NOUN
eurjchem-170	54	32	.	.	PUNCT
eurjchem-170	55	1	2.4	2.4	NUM
eurjchem-170	55	2	.	.	PUNCT
eurjchem-170	56	1	hplc	hplc	NOUN
eurjchem-170	56	2	method	method	PROPN
eurjchem-170	56	3	development	development	NOUN
eurjchem-170	56	4	the	the	DET
eurjchem-170	56	5	lc	lc	PROPN
eurjchem-170	56	6	column	column	NOUN
eurjchem-170	56	7	used	use	VERB
eurjchem-170	56	8	in	in	ADP
eurjchem-170	56	9	method	method	NOUN
eurjchem-170	56	10	development	development	NOUN
eurjchem-170	56	11	was	be	AUX
eurjchem-170	56	12	pursuit	pursuit	ADJ
eurjchem-170	56	13	xrs	xrs	PROPN
eurjchem-170	56	14	c‐8	c‐8	NOUN
eurjchem-170	56	15	(	(	PUNCT
eurjchem-170	56	16	250	250	NUM
eurjchem-170	56	17	mm	mm	NOUN
eurjchem-170	56	18	x	x	SYM
eurjchem-170	56	19	4.6	4.6	NUM
eurjchem-170	56	20	mm	mm	INTJ
eurjchem-170	56	21	i.d	i.d	PROPN
eurjchem-170	56	22	.	.	PROPN
eurjchem-170	56	23	,	,	PUNCT
eurjchem-170	56	24	particle	particle	NOUN
eurjchem-170	56	25	size	size	NOUN
eurjchem-170	56	26	5	5	NUM
eurjchem-170	56	27	m	m	PROPN
eurjchem-170	56	28	)	)	PUNCT
eurjchem-170	56	29	from	from	ADP
eurjchem-170	56	30	varian	varian	PROPN
eurjchem-170	56	31	(	(	PUNCT
eurjchem-170	56	32	ca	ca	PROPN
eurjchem-170	56	33	,	,	PUNCT
eurjchem-170	56	34	usa	usa	PROPN
eurjchem-170	56	35	)	)	PUNCT
eurjchem-170	56	36	.	.	PUNCT
eurjchem-170	57	1	the	the	DET
eurjchem-170	57	2	ratios	ratio	NOUN
eurjchem-170	57	3	of	of	ADP
eurjchem-170	57	4	organic	organic	ADJ
eurjchem-170	57	5	modifier	modifier	NOUN
eurjchem-170	57	6	(	(	PUNCT
eurjchem-170	57	7	acn	acn	PROPN
eurjchem-170	57	8	)	)	PUNCT
eurjchem-170	57	9	and	and	CCONJ
eurjchem-170	57	10	buffer	buffer	NOUN
eurjchem-170	57	11	(	(	PUNCT
eurjchem-170	57	12	potassium	potassium	NOUN
eurjchem-170	57	13	dihydrogen	dihydrogen	NOUN
eurjchem-170	57	14	phosphate	phosphate	NOUN
eurjchem-170	57	15	(	(	PUNCT
eurjchem-170	57	16	0.01	0.01	NUM
eurjchem-170	57	17	m	m	NOUN
eurjchem-170	57	18	;	;	PUNCT
eurjchem-170	57	19	ph	ph	X
eurjchem-170	57	20	3.0	3.0	NUM
eurjchem-170	57	21	)	)	PUNCT
eurjchem-170	57	22	)	)	PUNCT
eurjchem-170	57	23	were	be	AUX
eurjchem-170	57	24	varied	varied	ADJ
eurjchem-170	57	25	in	in	ADP
eurjchem-170	57	26	the	the	DET
eurjchem-170	57	27	mobile	mobile	ADJ
eurjchem-170	57	28	phase	phase	NOUN
eurjchem-170	57	29	to	to	PART
eurjchem-170	57	30	separate	separate	VERB
eurjchem-170	57	31	the	the	DET
eurjchem-170	57	32	drug	drug	NOUN
eurjchem-170	57	33	and	and	CCONJ
eurjchem-170	57	34	degradation	degradation	NOUN
eurjchem-170	57	35	product(s	product(s	PROPN
eurjchem-170	57	36	)	)	PUNCT
eurjchem-170	57	37	.	.	PUNCT
eurjchem-170	58	1	the	the	DET
eurjchem-170	58	2	buffer	buffer	NOUN
eurjchem-170	58	3	was	be	AUX
eurjchem-170	58	4	prepared	prepare	VERB
eurjchem-170	58	5	by	by	ADP
eurjchem-170	58	6	dissolving	dissolve	VERB
eurjchem-170	58	7	1.36	1.36	NUM
eurjchem-170	58	8	g	g	NOUN
eurjchem-170	58	9	of	of	ADP
eurjchem-170	58	10	anhydrous	anhydrous	ADJ
eurjchem-170	58	11	potassium	potassium	NOUN
eurjchem-170	58	12	dihydrogen	dihydrogen	NOUN
eurjchem-170	58	13	phosphate	phosphate	NOUN
eurjchem-170	58	14	in	in	ADP
eurjchem-170	58	15	1l	1l	NUM
eurjchem-170	58	16	water	water	NOUN
eurjchem-170	58	17	and	and	CCONJ
eurjchem-170	58	18	the	the	DET
eurjchem-170	58	19	ph	ph	NOUN
eurjchem-170	58	20	was	be	AUX
eurjchem-170	58	21	adjusted	adjust	VERB
eurjchem-170	58	22	using	use	VERB
eurjchem-170	58	23	phosphoric	phosphoric	ADJ
eurjchem-170	58	24	acid	acid	NOUN
eurjchem-170	58	25	.	.	PUNCT
eurjchem-170	59	1	the	the	DET
eurjchem-170	59	2	buffer	buffer	NOUN
eurjchem-170	59	3	ph	ph	NOUN
eurjchem-170	59	4	was	be	AUX
eurjchem-170	59	5	fixed	fix	VERB
eurjchem-170	59	6	as	as	ADP
eurjchem-170	59	7	3.0	3.0	NUM
eurjchem-170	59	8	considering	consider	VERB
eurjchem-170	59	9	the	the	DET
eurjchem-170	59	10	drug	drug	NOUN
eurjchem-170	59	11	’s	’s	PART
eurjchem-170	59	12	pka	pka	PROPN
eurjchem-170	59	13	values	value	NOUN
eurjchem-170	59	14	of	of	ADP
eurjchem-170	59	15	3.1	3.1	NUM
eurjchem-170	59	16	and	and	CCONJ
eurjchem-170	59	17	4.3	4.3	NUM
eurjchem-170	59	18	,	,	PUNCT
eurjchem-170	59	19	calculated	calculate	VERB
eurjchem-170	59	20	using	use	VERB
eurjchem-170	59	21	acd	acd	NOUN
eurjchem-170	59	22	software	software	NOUN
eurjchem-170	59	23	.	.	PUNCT
eurjchem-170	60	1	the	the	DET
eurjchem-170	60	2	mobile	mobile	ADJ
eurjchem-170	60	3	phase	phase	NOUN
eurjchem-170	60	4	components	component	NOUN
eurjchem-170	60	5	were	be	AUX
eurjchem-170	60	6	filtered	filter	VERB
eurjchem-170	60	7	through	through	ADP
eurjchem-170	60	8	0.45	0.45	NUM
eurjchem-170	60	9	μm	μm	NOUN
eurjchem-170	60	10	nylon	nylon	NOUN
eurjchem-170	60	11	filter	filter	NOUN
eurjchem-170	60	12	and	and	CCONJ
eurjchem-170	60	13	degassed	degas	VERB
eurjchem-170	60	14	before	before	ADP
eurjchem-170	60	15	use	use	NOUN
eurjchem-170	60	16	.	.	PUNCT
eurjchem-170	61	1	the	the	DET
eurjchem-170	61	2	injection	injection	NOUN
eurjchem-170	61	3	volume	volume	NOUN
eurjchem-170	61	4	and	and	CCONJ
eurjchem-170	61	5	flow	flow	NOUN
eurjchem-170	61	6	rate	rate	NOUN
eurjchem-170	61	7	were	be	AUX
eurjchem-170	61	8	10	10	NUM
eurjchem-170	61	9	μl	μl	ADP
eurjchem-170	61	10	and	and	CCONJ
eurjchem-170	61	11	1.0	1.0	NUM
eurjchem-170	61	12	ml	ml	NOUN
eurjchem-170	61	13	/	/	SYM
eurjchem-170	61	14	min	min	NOUN
eurjchem-170	61	15	,	,	PUNCT
eurjchem-170	61	16	respectively	respectively	ADV
eurjchem-170	61	17	.	.	PUNCT
eurjchem-170	62	1	all	all	DET
eurjchem-170	62	2	studies	study	NOUN
eurjchem-170	62	3	were	be	AUX
eurjchem-170	62	4	carried	carry	VERB
eurjchem-170	62	5	out	out	ADP
eurjchem-170	62	6	at	at	ADP
eurjchem-170	62	7	25	25	NUM
eurjchem-170	62	8	oc	oc	NOUN
eurjchem-170	62	9	.	.	PUNCT
eurjchem-170	63	1	the	the	DET
eurjchem-170	63	2	wavelength	wavelength	NOUN
eurjchem-170	63	3	of	of	ADP
eurjchem-170	63	4	detection	detection	NOUN
eurjchem-170	63	5	was	be	AUX
eurjchem-170	63	6	233	233	NUM
eurjchem-170	63	7	nm	nm	NOUN
eurjchem-170	63	8	.	.	PUNCT
eurjchem-170	64	1	2.5	2.5	NUM
eurjchem-170	64	2	.	.	PUNCT
eurjchem-170	65	1	ms	ms	PROPN
eurjchem-170	65	2	/	/	SYM
eurjchem-170	65	3	tof	tof	PROPN
eurjchem-170	65	4	,	,	PUNCT
eurjchem-170	65	5	msn	msn	NOUN
eurjchem-170	65	6	and	and	CCONJ
eurjchem-170	65	7	h	h	NOUN
eurjchem-170	65	8	/	/	SYM
eurjchem-170	65	9	d	d	PROPN
eurjchem-170	65	10	exchange	exchange	NOUN
eurjchem-170	65	11	studies	study	NOUN
eurjchem-170	65	12	on	on	ADP
eurjchem-170	65	13	the	the	DET
eurjchem-170	65	14	drug	drug	NOUN
eurjchem-170	65	15	ms	ms	PROPN
eurjchem-170	65	16	/	/	SYM
eurjchem-170	65	17	tof	tof	PROPN
eurjchem-170	65	18	studies	study	NOUN
eurjchem-170	65	19	were	be	AUX
eurjchem-170	65	20	performed	perform	VERB
eurjchem-170	65	21	in	in	ADP
eurjchem-170	65	22	esi	esi	PROPN
eurjchem-170	65	23	positive	positive	ADJ
eurjchem-170	65	24	mode	mode	NOUN
eurjchem-170	65	25	in	in	ADP
eurjchem-170	65	26	the	the	DET
eurjchem-170	65	27	mass	mass	ADJ
eurjchem-170	65	28	range	range	NOUN
eurjchem-170	65	29	of	of	ADP
eurjchem-170	65	30	50	50	NUM
eurjchem-170	65	31	to	to	PART
eurjchem-170	65	32	1500	1500	NUM
eurjchem-170	65	33	da	da	NOUN
eurjchem-170	65	34	.	.	PUNCT
eurjchem-170	66	1	the	the	DET
eurjchem-170	66	2	drug	drug	NOUN
eurjchem-170	66	3	was	be	AUX
eurjchem-170	66	4	also	also	ADV
eurjchem-170	66	5	subjected	subject	VERB
eurjchem-170	66	6	to	to	ADP
eurjchem-170	66	7	msn	msn	PROPN
eurjchem-170	66	8	study	study	NOUN
eurjchem-170	66	9	,	,	PUNCT
eurjchem-170	66	10	wherein	wherein	SCONJ
eurjchem-170	66	11	fragmentation	fragmentation	NOUN
eurjchem-170	66	12	of	of	ADP
eurjchem-170	66	13	various	various	ADJ
eurjchem-170	66	14	precursor	precursor	NOUN
eurjchem-170	66	15	ions	ion	NOUN
eurjchem-170	66	16	was	be	AUX
eurjchem-170	66	17	achieved	achieve	VERB
eurjchem-170	66	18	using	use	VERB
eurjchem-170	66	19	different	different	ADJ
eurjchem-170	66	20	collision	collision	NOUN
eurjchem-170	66	21	energies	energy	NOUN
eurjchem-170	66	22	.	.	PUNCT
eurjchem-170	67	1	mass	mass	ADJ
eurjchem-170	67	2	system	system	NOUN
eurjchem-170	67	3	parameters	parameter	NOUN
eurjchem-170	67	4	were	be	AUX
eurjchem-170	67	5	optimized	optimize	VERB
eurjchem-170	67	6	appropriately	appropriately	ADV
eurjchem-170	67	7	for	for	ADP
eurjchem-170	67	8	the	the	DET
eurjchem-170	67	9	above	above	ADJ
eurjchem-170	67	10	studies	study	NOUN
eurjchem-170	67	11	.	.	PUNCT
eurjchem-170	68	1	h	h	NOUN
eurjchem-170	68	2	/	/	SYM
eurjchem-170	68	3	d	d	PROPN
eurjchem-170	68	4	exchange	exchange	NOUN
eurjchem-170	68	5	was	be	AUX
eurjchem-170	68	6	carried	carry	VERB
eurjchem-170	68	7	out	out	ADP
eurjchem-170	68	8	on	on	ADP
eurjchem-170	68	9	the	the	DET
eurjchem-170	68	10	ms	ms	PROPN
eurjchem-170	68	11	/	/	SYM
eurjchem-170	68	12	tof	tof	PROPN
eurjchem-170	68	13	system	system	NOUN
eurjchem-170	68	14	by	by	ADP
eurjchem-170	68	15	direct	direct	ADJ
eurjchem-170	68	16	injection	injection	NOUN
eurjchem-170	68	17	of	of	ADP
eurjchem-170	68	18	a	a	DET
eurjchem-170	68	19	drug	drug	NOUN
eurjchem-170	68	20	solution	solution	NOUN
eurjchem-170	68	21	(	(	PUNCT
eurjchem-170	68	22	2	2	NUM
eurjchem-170	68	23	ppm	ppm	NOUN
eurjchem-170	68	24	)	)	PUNCT
eurjchem-170	68	25	in	in	ADP
eurjchem-170	68	26	acn	acn	PROPN
eurjchem-170	68	27	and	and	CCONJ
eurjchem-170	68	28	d2o	d2o	PROPN
eurjchem-170	68	29	(	(	PUNCT
eurjchem-170	68	30	50:50	50:50	NUM
eurjchem-170	68	31	,	,	PUNCT
eurjchem-170	68	32	v	v	NOUN
eurjchem-170	68	33	:	:	PUNCT
eurjchem-170	68	34	v	v	NOUN
eurjchem-170	68	35	)	)	PUNCT
eurjchem-170	68	36	.	.	PUNCT
eurjchem-170	69	1	2.6	2.6	NUM
eurjchem-170	69	2	.	.	PUNCT
eurjchem-170	69	3	lc‐ms	lc‐ms	AUX
eurjchem-170	69	4	/	/	SYM
eurjchem-170	69	5	tof	tof	PROPN
eurjchem-170	69	6	and	and	CCONJ
eurjchem-170	69	7	on‐line	on‐line	PROPN
eurjchem-170	69	8	h	h	NOUN
eurjchem-170	69	9	/	/	SYM
eurjchem-170	69	10	d	d	PROPN
eurjchem-170	69	11	exchange	exchange	NOUN
eurjchem-170	69	12	studies	study	NOUN
eurjchem-170	69	13	on	on	ADP
eurjchem-170	69	14	the	the	DET
eurjchem-170	69	15	product	product	NOUN
eurjchem-170	69	16	the	the	DET
eurjchem-170	69	17	drug	drug	NOUN
eurjchem-170	69	18	and	and	CCONJ
eurjchem-170	69	19	the	the	DET
eurjchem-170	69	20	stressed	stress	VERB
eurjchem-170	69	21	samples	sample	NOUN
eurjchem-170	69	22	were	be	AUX
eurjchem-170	69	23	subjected	subject	VERB
eurjchem-170	69	24	to	to	ADP
eurjchem-170	69	25	lc‐	lc‐	ADJ
eurjchem-170	69	26	ms	ms	PROPN
eurjchem-170	69	27	/	/	SYM
eurjchem-170	69	28	tof	tof	PROPN
eurjchem-170	69	29	studies	study	NOUN
eurjchem-170	69	30	using	use	VERB
eurjchem-170	69	31	the	the	DET
eurjchem-170	69	32	developed	develop	VERB
eurjchem-170	69	33	lc	lc	NOUN
eurjchem-170	69	34	method	method	NOUN
eurjchem-170	69	35	,	,	PUNCT
eurjchem-170	69	36	but	but	CCONJ
eurjchem-170	69	37	after	after	ADP
eurjchem-170	69	38	replacing	replace	VERB
eurjchem-170	69	39	phosphate	phosphate	ADJ
eurjchem-170	69	40	buffer	buffer	NOUN
eurjchem-170	69	41	with	with	ADP
eurjchem-170	69	42	ammonium	ammonium	NOUN
eurjchem-170	69	43	acetate	acetate	NOUN
eurjchem-170	69	44	having	have	VERB
eurjchem-170	69	45	same	same	ADJ
eurjchem-170	69	46	molarity	molarity	NOUN
eurjchem-170	69	47	and	and	CCONJ
eurjchem-170	69	48	ph	ph	NOUN
eurjchem-170	69	49	.	.	PROPN
eurjchem-170	69	50	for	for	ADP
eurjchem-170	69	51	internal	internal	ADJ
eurjchem-170	69	52	calibration	calibration	NOUN
eurjchem-170	69	53	,	,	PUNCT
eurjchem-170	69	54	the	the	DET
eurjchem-170	69	55	es	es	NOUN
eurjchem-170	69	56	tuning	tuning	NOUN
eurjchem-170	69	57	mix	mix	NOUN
eurjchem-170	69	58	solution	solution	NOUN
eurjchem-170	69	59	was	be	AUX
eurjchem-170	69	60	injected	inject	VERB
eurjchem-170	69	61	through	through	ADP
eurjchem-170	69	62	a	a	DET
eurjchem-170	69	63	diverter	diverter	NOUN
eurjchem-170	69	64	in	in	ADP
eurjchem-170	69	65	a	a	DET
eurjchem-170	69	66	specific	specific	ADJ
eurjchem-170	69	67	segment	segment	NOUN
eurjchem-170	69	68	near	near	ADP
eurjchem-170	69	69	the	the	DET
eurjchem-170	69	70	peak	peak	NOUN
eurjchem-170	69	71	of	of	ADP
eurjchem-170	69	72	interest	interest	NOUN
eurjchem-170	69	73	.	.	PUNCT
eurjchem-170	70	1	the	the	DET
eurjchem-170	70	2	on‐line	on‐line	PROPN
eurjchem-170	70	3	h	h	NOUN
eurjchem-170	70	4	/	/	SYM
eurjchem-170	70	5	d	d	PROPN
eurjchem-170	70	6	exchange	exchange	NOUN
eurjchem-170	70	7	mass	mass	NOUN
eurjchem-170	70	8	studies	study	NOUN
eurjchem-170	70	9	were	be	AUX
eurjchem-170	70	10	carried	carry	VERB
eurjchem-170	70	11	out	out	ADP
eurjchem-170	70	12	on	on	ADP
eurjchem-170	70	13	the	the	DET
eurjchem-170	70	14	ltq‐msn	ltq‐msn	PUNCT
eurjchem-170	70	15	system	system	NOUN
eurjchem-170	70	16	,	,	PUNCT
eurjchem-170	70	17	wherein	wherein	SCONJ
eurjchem-170	70	18	injection	injection	NOUN
eurjchem-170	70	19	of	of	ADP
eurjchem-170	70	20	d2o	d2o	PROPN
eurjchem-170	70	21	was	be	AUX
eurjchem-170	70	22	made	make	VERB
eurjchem-170	70	23	via	via	ADP
eurjchem-170	70	24	an	an	DET
eurjchem-170	70	25	additional	additional	ADJ
eurjchem-170	70	26	channel	channel	NOUN
eurjchem-170	70	27	,	,	PUNCT
eurjchem-170	70	28	just	just	ADV
eurjchem-170	70	29	before	before	SCONJ
eurjchem-170	70	30	the	the	DET
eurjchem-170	70	31	peak	peak	NOUN
eurjchem-170	70	32	of	of	ADP
eurjchem-170	70	33	interest	interest	NOUN
eurjchem-170	70	34	started	start	VERB
eurjchem-170	70	35	eluting	elute	VERB
eurjchem-170	70	36	from	from	ADP
eurjchem-170	70	37	the	the	DET
eurjchem-170	70	38	column	column	NOUN
eurjchem-170	70	39	.	.	PUNCT
eurjchem-170	71	1	the	the	DET
eurjchem-170	71	2	flow	flow	NOUN
eurjchem-170	71	3	of	of	ADP
eurjchem-170	71	4	d2o	d2o	PROPN
eurjchem-170	71	5	was	be	AUX
eurjchem-170	71	6	continued	continue	VERB
eurjchem-170	71	7	until	until	SCONJ
eurjchem-170	71	8	the	the	DET
eurjchem-170	71	9	peak	peak	NOUN
eurjchem-170	71	10	was	be	AUX
eurjchem-170	71	11	completely	completely	ADV
eurjchem-170	71	12	eluted	elute	VERB
eurjchem-170	71	13	.	.	PUNCT
eurjchem-170	72	1	2.7	2.7	NUM
eurjchem-170	72	2	.	.	PUNCT
eurjchem-170	73	1	lc‐nmr	lc‐nmr	ADJ
eurjchem-170	73	2	studies	study	NOUN
eurjchem-170	73	3	on	on	ADP
eurjchem-170	73	4	the	the	DET
eurjchem-170	73	5	drug	drug	NOUN
eurjchem-170	73	6	and	and	CCONJ
eurjchem-170	73	7	the	the	DET
eurjchem-170	73	8	product	product	NOUN
eurjchem-170	73	9	for	for	ADP
eurjchem-170	73	10	lc‐nmr	lc‐nmr	PROPN
eurjchem-170	73	11	studies	study	NOUN
eurjchem-170	73	12	,	,	PUNCT
eurjchem-170	73	13	the	the	DET
eurjchem-170	73	14	photolytic	photolytic	ADJ
eurjchem-170	73	15	stressed	stress	VERB
eurjchem-170	73	16	sample	sample	NOUN
eurjchem-170	73	17	was	be	AUX
eurjchem-170	73	18	subjected	subject	VERB
eurjchem-170	73	19	to	to	ADP
eurjchem-170	73	20	lc	lc	NOUN
eurjchem-170	73	21	using	use	VERB
eurjchem-170	73	22	the	the	DET
eurjchem-170	73	23	same	same	ADJ
eurjchem-170	73	24	mobile	mobile	ADJ
eurjchem-170	73	25	phase	phase	NOUN
eurjchem-170	73	26	as	as	SCONJ
eurjchem-170	73	27	used	use	VERB
eurjchem-170	73	28	for	for	ADP
eurjchem-170	73	29	hplc	hplc	NOUN
eurjchem-170	73	30	,	,	PUNCT
eurjchem-170	73	31	but	but	CCONJ
eurjchem-170	73	32	using	use	VERB
eurjchem-170	73	33	d2o	d2o	PROPN
eurjchem-170	73	34	instead	instead	ADV
eurjchem-170	73	35	of	of	ADP
eurjchem-170	73	36	water	water	NOUN
eurjchem-170	73	37	.	.	PUNCT
eurjchem-170	74	1	the	the	DET
eurjchem-170	74	2	separated	separate	VERB
eurjchem-170	74	3	product	product	NOUN
eurjchem-170	74	4	was	be	AUX
eurjchem-170	74	5	collected	collect	VERB
eurjchem-170	74	6	in	in	ADP
eurjchem-170	74	7	the	the	DET
eurjchem-170	74	8	fraction	fraction	NOUN
eurjchem-170	74	9	loop	loop	NOUN
eurjchem-170	74	10	using	use	VERB
eurjchem-170	74	11	terminal	terminal	ADJ
eurjchem-170	74	12	cube	cube	NOUN
eurjchem-170	74	13	and	and	CCONJ
eurjchem-170	74	14	sent	send	VERB
eurjchem-170	74	15	to	to	PART
eurjchem-170	74	16	inverse	inverse	VERB
eurjchem-170	74	17	3	3	NUM
eurjchem-170	74	18	mm	mm	PROPN
eurjchem-170	74	19	nmr	nmr	NOUN
eurjchem-170	74	20	flow	flow	NOUN
eurjchem-170	74	21	probe	probe	NOUN
eurjchem-170	74	22	equipped	equip	VERB
eurjchem-170	74	23	with	with	ADP
eurjchem-170	74	24	1h	1h	NUM
eurjchem-170	74	25	{	{	PUNCT
eurjchem-170	74	26	13c	13c	NOUN
eurjchem-170	74	27	}	}	PUNCT
eurjchem-170	74	28	channels	channel	NOUN
eurjchem-170	74	29	with	with	ADP
eurjchem-170	74	30	pulsed‐field	pulsed‐field	ADJ
eurjchem-170	74	31	gradient	gradient	NOUN
eurjchem-170	74	32	along	along	ADP
eurjchem-170	74	33	z‐axis	z‐axis	PROPN
eurjchem-170	74	34	.	.	PUNCT
eurjchem-170	75	1	the	the	DET
eurjchem-170	75	2	active	active	ADJ
eurjchem-170	75	3	sample	sample	NOUN
eurjchem-170	75	4	volume	volume	NOUN
eurjchem-170	75	5	of	of	ADP
eurjchem-170	75	6	the	the	DET
eurjchem-170	75	7	probe	probe	NOUN
eurjchem-170	75	8	was	be	AUX
eurjchem-170	75	9	approximately	approximately	ADV
eurjchem-170	75	10	60	60	NUM
eurjchem-170	75	11	μl	μl	ADV
eurjchem-170	75	12	and	and	CCONJ
eurjchem-170	75	13	the	the	DET
eurjchem-170	75	14	transfer	transfer	NOUN
eurjchem-170	75	15	time	time	NOUN
eurjchem-170	75	16	from	from	ADP
eurjchem-170	75	17	uv	uv	NOUN
eurjchem-170	75	18	cell	cell	NOUN
eurjchem-170	75	19	to	to	ADP
eurjchem-170	75	20	the	the	DET
eurjchem-170	75	21	active	active	ADJ
eurjchem-170	75	22	volume	volume	NOUN
eurjchem-170	75	23	was	be	AUX
eurjchem-170	75	24	45	45	NUM
eurjchem-170	75	25	s	s	NOUN
eurjchem-170	75	26	at	at	ADP
eurjchem-170	75	27	a	a	DET
eurjchem-170	75	28	flow‐rate	flow‐rate	NOUN
eurjchem-170	75	29	of	of	ADP
eurjchem-170	75	30	0.5	0.5	NUM
eurjchem-170	75	31	ml	ml	NOUN
eurjchem-170	75	32	/	/	SYM
eurjchem-170	75	33	min	min	NOUN
eurjchem-170	75	34	.	.	NOUN
eurjchem-170	75	35	one	one	NUM
eurjchem-170	75	36	dimensional	dimensional	ADJ
eurjchem-170	75	37	1h	1h	NUM
eurjchem-170	75	38	spectra	spectra	NOUN
eurjchem-170	75	39	were	be	AUX
eurjchem-170	75	40	recorded	record	VERB
eurjchem-170	75	41	using	use	VERB
eurjchem-170	75	42	the	the	DET
eurjchem-170	75	43	wet	wet	ADJ
eurjchem-170	75	44	pulse	pulse	NOUN
eurjchem-170	75	45	sequences	sequence	NOUN
eurjchem-170	75	46	for	for	ADP
eurjchem-170	75	47	solvent	solvent	ADJ
eurjchem-170	75	48	suppression	suppression	NOUN
eurjchem-170	75	49	of	of	ADP
eurjchem-170	75	50	acn	acn	PROPN
eurjchem-170	75	51	and	and	CCONJ
eurjchem-170	75	52	residual	residual	ADJ
eurjchem-170	75	53	hod	hod	PROPN
eurjchem-170	75	54	signal	signal	NOUN
eurjchem-170	75	55	,	,	PUNCT
eurjchem-170	75	56	with	with	ADP
eurjchem-170	75	57	attenuated	attenuate	VERB
eurjchem-170	75	58	power	power	NOUN
eurjchem-170	75	59	at	at	ADP
eurjchem-170	75	60	64.5	64.5	NUM
eurjchem-170	75	61	[	[	X
eurjchem-170	75	62	db	db	X
eurjchem-170	75	63	]	]	X
eurjchem-170	75	64	,	,	PUNCT
eurjchem-170	75	65	which	which	PRON
eurjchem-170	75	66	gave	give	VERB
eurjchem-170	75	67	digital	digital	ADJ
eurjchem-170	75	68	resolution	resolution	NOUN
eurjchem-170	75	69	of	of	ADP
eurjchem-170	75	70	0.76	0.76	NUM
eurjchem-170	75	71	hz	hz	NOUN
eurjchem-170	75	72	per	per	ADP
eurjchem-170	75	73	point	point	NOUN
eurjchem-170	75	74	for	for	ADP
eurjchem-170	75	75	the	the	DET
eurjchem-170	75	76	product	product	NOUN
eurjchem-170	75	77	.	.	PUNCT
eurjchem-170	76	1	the	the	DET
eurjchem-170	76	2	spectra	spectra	NOUN
eurjchem-170	76	3	were	be	AUX
eurjchem-170	76	4	acquired	acquire	VERB
eurjchem-170	76	5	with	with	ADP
eurjchem-170	76	6	16	16	NUM
eurjchem-170	76	7	khz	khz	NOUN
eurjchem-170	76	8	spectral	spectral	ADJ
eurjchem-170	76	9	width	width	NOUN
eurjchem-170	76	10	,	,	PUNCT
eurjchem-170	76	11	16	16	NUM
eurjchem-170	76	12	k	k	PROPN
eurjchem-170	76	13	data	datum	NOUN
eurjchem-170	76	14	points	point	NOUN
eurjchem-170	76	15	and	and	CCONJ
eurjchem-170	76	16	1024	1024	NUM
eurjchem-170	76	17	scans	scan	NOUN
eurjchem-170	76	18	.	.	PUNCT
eurjchem-170	77	1	the	the	DET
eurjchem-170	77	2	drug	drug	NOUN
eurjchem-170	77	3	solution	solution	NOUN
eurjchem-170	77	4	(	(	PUNCT
eurjchem-170	77	5	4	4	NUM
eurjchem-170	77	6	mg	mg	NUM
eurjchem-170	77	7	/	/	SYM
eurjchem-170	77	8	ml	ml	NOUN
eurjchem-170	77	9	)	)	PUNCT
eurjchem-170	77	10	was	be	AUX
eurjchem-170	77	11	prepared	prepare	VERB
eurjchem-170	77	12	in	in	ADP
eurjchem-170	77	13	the	the	DET
eurjchem-170	77	14	mobile	mobile	ADJ
eurjchem-170	77	15	phase	phase	NOUN
eurjchem-170	77	16	and	and	CCONJ
eurjchem-170	77	17	directly	directly	ADV
eurjchem-170	77	18	injected	inject	VERB
eurjchem-170	77	19	to	to	ADP
eurjchem-170	77	20	lc‐nmr	lc‐nmr	ADJ
eurjchem-170	77	21	probe	probe	NOUN
eurjchem-170	77	22	.	.	PUNCT
eurjchem-170	78	1	the	the	DET
eurjchem-170	78	2	cosy	cosy	ADJ
eurjchem-170	78	3	spectra	spectra	NOUN
eurjchem-170	78	4	of	of	ADP
eurjchem-170	78	5	the	the	DET
eurjchem-170	78	6	drug	drug	NOUN
eurjchem-170	78	7	and	and	CCONJ
eurjchem-170	78	8	its	its	PRON
eurjchem-170	78	9	product	product	NOUN
eurjchem-170	78	10	were	be	AUX
eurjchem-170	78	11	acquired	acquire	VERB
eurjchem-170	78	12	using	use	VERB
eurjchem-170	78	13	wet	wet	ADJ
eurjchem-170	78	14	pulse	pulse	NOUN
eurjchem-170	78	15	sequences	sequence	NOUN
eurjchem-170	78	16	for	for	ADP
eurjchem-170	78	17	solvent	solvent	ADJ
eurjchem-170	78	18	suppression	suppression	NOUN
eurjchem-170	78	19	.	.	PUNCT
eurjchem-170	79	1	a	a	DET
eurjchem-170	79	2	total	total	NOUN
eurjchem-170	79	3	of	of	ADP
eurjchem-170	79	4	96	96	NUM
eurjchem-170	79	5	scans	scan	NOUN
eurjchem-170	79	6	were	be	AUX
eurjchem-170	79	7	collected	collect	VERB
eurjchem-170	79	8	at	at	ADP
eurjchem-170	79	9	256	256	NUM
eurjchem-170	79	10	iterations	iteration	NOUN
eurjchem-170	79	11	in	in	ADP
eurjchem-170	79	12	the	the	DET
eurjchem-170	79	13	f1	f1	PROPN
eurjchem-170	79	14	dimension	dimension	NOUN
eurjchem-170	79	15	,	,	PUNCT
eurjchem-170	79	16	using	use	VERB
eurjchem-170	79	17	a	a	DET
eurjchem-170	79	18	spectral	spectral	ADJ
eurjchem-170	79	19	width	width	NOUN
eurjchem-170	79	20	of	of	ADP
eurjchem-170	79	21	~10	~10	X
eurjchem-170	79	22	khz	khz	NOUN
eurjchem-170	79	23	in	in	ADP
eurjchem-170	79	24	both	both	DET
eurjchem-170	79	25	dimensions	dimension	NOUN
eurjchem-170	79	26	.	.	PUNCT
eurjchem-170	80	1	it	it	PRON
eurjchem-170	80	2	was	be	AUX
eurjchem-170	80	3	found	find	VERB
eurjchem-170	80	4	that	that	SCONJ
eurjchem-170	80	5	traces	trace	NOUN
eurjchem-170	80	6	of	of	ADP
eurjchem-170	80	7	methanol	methanol	NOUN
eurjchem-170	80	8	were	be	AUX
eurjchem-170	80	9	present	present	ADJ
eurjchem-170	80	10	as	as	ADP
eurjchem-170	80	11	an	an	DET
eurjchem-170	80	12	impurity	impurity	NOUN
eurjchem-170	80	13	in	in	ADP
eurjchem-170	80	14	the	the	DET
eurjchem-170	80	15	mobile	mobile	ADJ
eurjchem-170	80	16	phase	phase	NOUN
eurjchem-170	80	17	.	.	PUNCT
eurjchem-170	81	1	therefore	therefore	ADV
eurjchem-170	81	2	,	,	PUNCT
eurjchem-170	81	3	the	the	DET
eurjchem-170	81	4	chemical	chemical	ADJ
eurjchem-170	81	5	shifts	shift	NOUN
eurjchem-170	81	6	of	of	ADP
eurjchem-170	81	7	1h	1h	NUM
eurjchem-170	81	8	signals	signal	NOUN
eurjchem-170	81	9	were	be	AUX
eurjchem-170	81	10	referenced	reference	VERB
eurjchem-170	81	11	to	to	ADP
eurjchem-170	81	12	the	the	DET
eurjchem-170	81	13	methoxy	methoxy	ADJ
eurjchem-170	81	14	signal	signal	NOUN
eurjchem-170	81	15	of	of	ADP
eurjchem-170	81	16	the	the	DET
eurjchem-170	81	17	residual	residual	ADJ
eurjchem-170	81	18	ch3oh	ch3oh	NOUN
eurjchem-170	81	19	at	at	ADP
eurjchem-170	81	20	δ	δ	PROPN
eurjchem-170	81	21	3.30	3.30	NUM
eurjchem-170	81	22	ppm	ppm	NOUN
eurjchem-170	81	23	.	.	PUNCT
eurjchem-170	82	1	3	3	X
eurjchem-170	82	2	.	.	NOUN
eurjchem-170	82	3	results	result	NOUN
eurjchem-170	82	4	and	and	CCONJ
eurjchem-170	82	5	discussion	discussion	NOUN
eurjchem-170	82	6	3.1	3.1	NUM
eurjchem-170	82	7	.	.	PUNCT
eurjchem-170	83	1	hplc	hplc	NOUN
eurjchem-170	83	2	method	method	VERB
eurjchem-170	83	3	all	all	DET
eurjchem-170	83	4	the	the	DET
eurjchem-170	83	5	stressed	stress	VERB
eurjchem-170	83	6	solutions	solution	NOUN
eurjchem-170	83	7	were	be	AUX
eurjchem-170	83	8	initially	initially	ADV
eurjchem-170	83	9	analyzed	analyze	VERB
eurjchem-170	83	10	by	by	ADP
eurjchem-170	83	11	hplc	hplc	NOUN
eurjchem-170	83	12	using	use	VERB
eurjchem-170	83	13	acn	acn	PROPN
eurjchem-170	83	14	(	(	PUNCT
eurjchem-170	83	15	a	a	NOUN
eurjchem-170	83	16	)	)	PUNCT
eurjchem-170	83	17	and	and	CCONJ
eurjchem-170	83	18	potassium	potassium	NOUN
eurjchem-170	83	19	dihydrogen	dihydrogen	NOUN
eurjchem-170	83	20	phosphate	phosphate	NOUN
eurjchem-170	83	21	(	(	PUNCT
eurjchem-170	83	22	b	b	NOUN
eurjchem-170	83	23	)	)	PUNCT
eurjchem-170	83	24	in	in	ADP
eurjchem-170	83	25	the	the	DET
eurjchem-170	83	26	following	follow	VERB
eurjchem-170	83	27	same	same	ADJ
eurjchem-170	83	28	gradient	gradient	ADJ
eurjchem-170	83	29	mode	mode	NOUN
eurjchem-170	83	30	:	:	PUNCT
eurjchem-170	83	31	tmin	tmin	NOUN
eurjchem-170	83	32	/	/	SYM
eurjchem-170	83	33	a	a	DET
eurjchem-170	83	34	:	:	PUNCT
eurjchem-170	83	35	b	b	NOUN
eurjchem-170	83	36	;	;	PUNCT
eurjchem-170	83	37	t0‐1/10:90	t0‐1/10:90	NUM
eurjchem-170	83	38	;	;	PUNCT
eurjchem-170	83	39	t60‐	t60‐	PROPN
eurjchem-170	83	40	70/90:10	70/90:10	NUM
eurjchem-170	83	41	;	;	PUNCT
eurjchem-170	83	42	t75‐82/10:90	t75‐82/10:90	NUM
eurjchem-170	83	43	.	.	PUNCT
eurjchem-170	84	1	except	except	SCONJ
eurjchem-170	84	2	,	,	PUNCT
eurjchem-170	84	3	frontal	frontal	ADJ
eurjchem-170	84	4	hump	hump	NOUN
eurjchem-170	84	5	in	in	ADP
eurjchem-170	84	6	the	the	DET
eurjchem-170	84	7	drug	drug	NOUN
eurjchem-170	84	8	peak	peak	NOUN
eurjchem-170	84	9	in	in	ADP
eurjchem-170	84	10	alkali	alkali	ADJ
eurjchem-170	84	11	solution	solution	NOUN
eurjchem-170	84	12	exposed	expose	VERB
eurjchem-170	84	13	to	to	ADP
eurjchem-170	84	14	light	light	NOUN
eurjchem-170	84	15	,	,	PUNCT
eurjchem-170	84	16	a	a	DET
eurjchem-170	84	17	sharp	sharp	ADJ
eurjchem-170	84	18	single	single	ADJ
eurjchem-170	84	19	drug	drug	NOUN
eurjchem-170	84	20	peak	peak	NOUN
eurjchem-170	84	21	was	be	AUX
eurjchem-170	84	22	observed	observe	VERB
eurjchem-170	84	23	in	in	ADP
eurjchem-170	84	24	all	all	DET
eurjchem-170	84	25	other	other	ADJ
eurjchem-170	84	26	stressed	stressed	ADJ
eurjchem-170	84	27	solutions	solution	NOUN
eurjchem-170	84	28	.	.	PUNCT
eurjchem-170	85	1	this	this	PRON
eurjchem-170	85	2	indicated	indicate	VERB
eurjchem-170	85	3	that	that	SCONJ
eurjchem-170	85	4	the	the	DET
eurjchem-170	85	5	drug	drug	NOUN
eurjchem-170	85	6	was	be	AUX
eurjchem-170	85	7	stable	stable	ADJ
eurjchem-170	85	8	to	to	ADP
eurjchem-170	85	9	all	all	DET
eurjchem-170	85	10	the	the	DET
eurjchem-170	85	11	stress	stress	NOUN
eurjchem-170	85	12	conditions	condition	NOUN
eurjchem-170	85	13	except	except	SCONJ
eurjchem-170	85	14	photo	photo	NOUN
eurjchem-170	85	15	alkali	alkali	PROPN
eurjchem-170	85	16	.	.	PUNCT
eurjchem-170	86	1	to	to	PART
eurjchem-170	86	2	separate	separate	VERB
eurjchem-170	86	3	the	the	DET
eurjchem-170	86	4	overlapping	overlap	VERB
eurjchem-170	86	5	product	product	NOUN
eurjchem-170	86	6	in	in	ADP
eurjchem-170	86	7	photo	photo	NOUN
eurjchem-170	86	8	alkaline	alkaline	NOUN
eurjchem-170	86	9	condition	condition	NOUN
eurjchem-170	86	10	,	,	PUNCT
eurjchem-170	86	11	the	the	DET
eurjchem-170	86	12	method	method	NOUN
eurjchem-170	86	13	was	be	AUX
eurjchem-170	86	14	improved	improve	VERB
eurjchem-170	86	15	by	by	ADP
eurjchem-170	86	16	varying	vary	VERB
eurjchem-170	86	17	the	the	DET
eurjchem-170	86	18	gradient	gradient	NOUN
eurjchem-170	86	19	.	.	PUNCT
eurjchem-170	87	1	the	the	DET
eurjchem-170	87	2	desired	desire	VERB
eurjchem-170	87	3	resolution	resolution	NOUN
eurjchem-170	87	4	(	(	PUNCT
eurjchem-170	87	5	rs	rs	INTJ
eurjchem-170	87	6	>	>	X
eurjchem-170	87	7	1.5	1.5	NUM
eurjchem-170	87	8	)	)	PUNCT
eurjchem-170	87	9	was	be	AUX
eurjchem-170	87	10	achieved	achieve	VERB
eurjchem-170	87	11	between	between	ADP
eurjchem-170	87	12	the	the	DET
eurjchem-170	87	13	degradation	degradation	NOUN
eurjchem-170	87	14	product	product	NOUN
eurjchem-170	87	15	and	and	CCONJ
eurjchem-170	87	16	the	the	DET
eurjchem-170	87	17	drug	drug	NOUN
eurjchem-170	87	18	by	by	ADP
eurjchem-170	87	19	using	use	VERB
eurjchem-170	87	20	the	the	DET
eurjchem-170	87	21	gradient	gradient	NOUN
eurjchem-170	87	22	:	:	PUNCT
eurjchem-170	87	23	tmin	tmin	NOUN
eurjchem-170	87	24	/	/	SYM
eurjchem-170	87	25	a	a	DET
eurjchem-170	87	26	:	:	PUNCT
eurjchem-170	87	27	b	b	NOUN
eurjchem-170	87	28	;	;	PUNCT
eurjchem-170	87	29	t0‐4/18:82	t0‐4/18:82	PROPN
eurjchem-170	87	30	;	;	PUNCT
eurjchem-170	87	31	t18/29:71	t18/29:71	NOUN
eurjchem-170	87	32	;	;	PUNCT
eurjchem-170	87	33	t22/30:70	t22/30:70	PROPN
eurjchem-170	87	34	;	;	PUNCT
eurjchem-170	87	35	t25/18:82	t25/18:82	PROPN
eurjchem-170	87	36	.	.	PUNCT
eurjchem-170	88	1	the	the	DET
eurjchem-170	88	2	chromatogram	chromatogram	NOUN
eurjchem-170	88	3	in	in	ADP
eurjchem-170	88	4	figure	figure	NOUN
eurjchem-170	88	5	1	1	NUM
eurjchem-170	88	6	depicts	depict	VERB
eurjchem-170	88	7	the	the	DET
eurjchem-170	88	8	separation	separation	NOUN
eurjchem-170	88	9	between	between	ADP
eurjchem-170	88	10	the	the	DET
eurjchem-170	88	11	two	two	NUM
eurjchem-170	88	12	components	component	NOUN
eurjchem-170	88	13	.	.	PUNCT
eurjchem-170	89	1	during	during	ADP
eurjchem-170	89	2	the	the	DET
eurjchem-170	89	3	course	course	NOUN
eurjchem-170	89	4	of	of	ADP
eurjchem-170	89	5	studies	study	NOUN
eurjchem-170	89	6	,	,	PUNCT
eurjchem-170	89	7	it	it	PRON
eurjchem-170	89	8	was	be	AUX
eurjchem-170	89	9	found	find	VERB
eurjchem-170	89	10	that	that	SCONJ
eurjchem-170	89	11	the	the	DET
eurjchem-170	89	12	degradation	degradation	NOUN
eurjchem-170	89	13	product	product	NOUN
eurjchem-170	89	14	was	be	AUX
eurjchem-170	89	15	stable	stable	ADJ
eurjchem-170	89	16	during	during	ADP
eurjchem-170	89	17	sample	sample	NOUN
eurjchem-170	89	18	handling	handling	NOUN
eurjchem-170	89	19	and	and	CCONJ
eurjchem-170	89	20	subsequent	subsequent	ADJ
eurjchem-170	89	21	analysis	analysis	NOUN
eurjchem-170	89	22	.	.	PUNCT
eurjchem-170	90	1	154	154	NUM
eurjchem-170	90	2	shah	shah	PROPN
eurjchem-170	90	3	et	et	PROPN
eurjchem-170	90	4	al	al	PROPN
eurjchem-170	90	5	.	.	PUNCT
eurjchem-170	90	6	/	/	SYM
eurjchem-170	90	7	european	european	PROPN
eurjchem-170	90	8	journal	journal	PROPN
eurjchem-170	90	9	of	of	ADP
eurjchem-170	90	10	chemistry	chemistry	NOUN
eurjchem-170	90	11	2	2	NUM
eurjchem-170	90	12	(	(	PUNCT
eurjchem-170	90	13	2	2	NUM
eurjchem-170	90	14	)	)	PUNCT
eurjchem-170	90	15	(	(	PUNCT
eurjchem-170	90	16	2011	2011	NUM
eurjchem-170	90	17	)	)	PUNCT
eurjchem-170	90	18	152‐157	152‐157	NUM
eurjchem-170	90	19	figure	figure	NOUN
eurjchem-170	90	20	1	1	NUM
eurjchem-170	90	21	.	.	PUNCT
eurjchem-170	91	1	hplc	hplc	NOUN
eurjchem-170	91	2	chromatogram	chromatogram	PROPN
eurjchem-170	91	3	showing	show	VERB
eurjchem-170	91	4	separation	separation	NOUN
eurjchem-170	91	5	of	of	ADP
eurjchem-170	91	6	the	the	DET
eurjchem-170	91	7	drug	drug	NOUN
eurjchem-170	91	8	and	and	CCONJ
eurjchem-170	91	9	the	the	DET
eurjchem-170	91	10	product	product	NOUN
eurjchem-170	91	11	.	.	PUNCT
eurjchem-170	92	1	3.2	3.2	NUM
eurjchem-170	92	2	.	.	NUM
eurjchem-170	92	3	optimized	optimize	VERB
eurjchem-170	92	4	mass	mass	NOUN
eurjchem-170	92	5	parameters	parameter	NOUN
eurjchem-170	92	6	to	to	PART
eurjchem-170	92	7	get	get	VERB
eurjchem-170	92	8	an	an	DET
eurjchem-170	92	9	optimal	optimal	ADJ
eurjchem-170	92	10	mass	mass	NOUN
eurjchem-170	92	11	spectrum	spectrum	NOUN
eurjchem-170	92	12	,	,	PUNCT
eurjchem-170	92	13	the	the	DET
eurjchem-170	92	14	selected	select	VERB
eurjchem-170	92	15	parameters	parameter	NOUN
eurjchem-170	92	16	for	for	ADP
eurjchem-170	92	17	ms	ms	PROPN
eurjchem-170	92	18	/	/	SYM
eurjchem-170	92	19	tof	tof	PROPN
eurjchem-170	92	20	system	system	NOUN
eurjchem-170	92	21	were	be	AUX
eurjchem-170	92	22	:	:	PUNCT
eurjchem-170	92	23	end	end	NOUN
eurjchem-170	92	24	plate	plate	NOUN
eurjchem-170	92	25	offset	offset	NOUN
eurjchem-170	92	26	,	,	PUNCT
eurjchem-170	92	27	‐500	‐500	PROPN
eurjchem-170	92	28	v	v	NOUN
eurjchem-170	92	29	;	;	PUNCT
eurjchem-170	92	30	capillary	capillary	ADJ
eurjchem-170	92	31	voltage	voltage	NOUN
eurjchem-170	92	32	,	,	PUNCT
eurjchem-170	92	33	‐4500	‐4500	NOUN
eurjchem-170	92	34	v	v	NOUN
eurjchem-170	92	35	;	;	PUNCT
eurjchem-170	92	36	nebuliser	nebuliser	NOUN
eurjchem-170	92	37	gas	gas	NOUN
eurjchem-170	92	38	pressure	pressure	NOUN
eurjchem-170	92	39	,	,	PUNCT
eurjchem-170	92	40	1.2	1.2	NUM
eurjchem-170	92	41	bar	bar	NOUN
eurjchem-170	92	42	;	;	PUNCT
eurjchem-170	92	43	dry	dry	ADJ
eurjchem-170	92	44	gas	gas	NOUN
eurjchem-170	92	45	flow	flow	NOUN
eurjchem-170	92	46	,	,	PUNCT
eurjchem-170	92	47	6.0	6.0	NUM
eurjchem-170	92	48	l	l	NOUN
eurjchem-170	92	49	/	/	SYM
eurjchem-170	92	50	min	min	NOUN
eurjchem-170	92	51	;	;	PUNCT
eurjchem-170	92	52	dry	dry	ADJ
eurjchem-170	92	53	temperature	temperature	NOUN
eurjchem-170	92	54	,	,	PUNCT
eurjchem-170	92	55	200	200	NUM
eurjchem-170	92	56	°	°	NOUN
eurjchem-170	92	57	c	c	NOUN
eurjchem-170	92	58	;	;	PUNCT
eurjchem-170	92	59	funnel	funnel	VERB
eurjchem-170	92	60	1	1	NUM
eurjchem-170	92	61	rf	rf	NOUN
eurjchem-170	92	62	,	,	PUNCT
eurjchem-170	92	63	150	150	NUM
eurjchem-170	92	64	vpp	vpp	NOUN
eurjchem-170	92	65	;	;	PUNCT
eurjchem-170	92	66	funnel	funnel	VERB
eurjchem-170	92	67	2	2	NUM
eurjchem-170	92	68	rf	rf	NOUN
eurjchem-170	92	69	,	,	PUNCT
eurjchem-170	92	70	300	300	NUM
eurjchem-170	92	71	vpp	vpp	NOUN
eurjchem-170	92	72	;	;	PUNCT
eurjchem-170	92	73	iscid	iscid	ADJ
eurjchem-170	92	74	energy	energy	NOUN
eurjchem-170	92	75	,	,	PUNCT
eurjchem-170	92	76	0.0	0.0	NUM
eurjchem-170	92	77	ev	ev	NOUN
eurjchem-170	92	78	;	;	PUNCT
eurjchem-170	92	79	hexapole	hexapole	NOUN
eurjchem-170	92	80	rf	rf	NOUN
eurjchem-170	92	81	,	,	PUNCT
eurjchem-170	92	82	120	120	NUM
eurjchem-170	92	83	vpp	vpp	NOUN
eurjchem-170	92	84	;	;	PUNCT
eurjchem-170	92	85	quadrupole	quadrupole	NOUN
eurjchem-170	92	86	ion	ion	NOUN
eurjchem-170	92	87	energy	energy	NOUN
eurjchem-170	92	88	,	,	PUNCT
eurjchem-170	92	89	4.0	4.0	NUM
eurjchem-170	92	90	ev	ev	NOUN
eurjchem-170	92	91	/	/	SYM
eurjchem-170	92	92	z	z	PROPN
eurjchem-170	92	93	;	;	PUNCT
eurjchem-170	92	94	collision	collision	NOUN
eurjchem-170	92	95	energy	energy	NOUN
eurjchem-170	92	96	,	,	PUNCT
eurjchem-170	92	97	22.0	22.0	NUM
eurjchem-170	92	98	ev	ev	PART
eurjchem-170	92	99	/	/	SYM
eurjchem-170	92	100	z	z	PROPN
eurjchem-170	92	101	;	;	PUNCT
eurjchem-170	92	102	transfer	transfer	NOUN
eurjchem-170	92	103	time	time	NOUN
eurjchem-170	92	104	,	,	PUNCT
eurjchem-170	92	105	50	50	NUM
eurjchem-170	92	106	µs	µs	NOUN
eurjchem-170	92	107	;	;	PUNCT
eurjchem-170	92	108	collision	collision	NOUN
eurjchem-170	92	109	rf	rf	NOUN
eurjchem-170	92	110	,	,	PUNCT
eurjchem-170	92	111	200	200	NUM
eurjchem-170	92	112	vpp	vpp	NOUN
eurjchem-170	92	113	,	,	PUNCT
eurjchem-170	92	114	and	and	CCONJ
eurjchem-170	92	115	pre‐pulse	pre‐pulse	NUM
eurjchem-170	92	116	storage	storage	NOUN
eurjchem-170	92	117	,	,	PUNCT
eurjchem-170	92	118	10	10	NUM
eurjchem-170	92	119	µs	µs	NOUN
eurjchem-170	92	120	.	.	PUNCT
eurjchem-170	93	1	similarly	similarly	ADV
eurjchem-170	93	2	,	,	PUNCT
eurjchem-170	93	3	the	the	DET
eurjchem-170	93	4	tuned	tune	VERB
eurjchem-170	93	5	parameters	parameter	NOUN
eurjchem-170	93	6	for	for	ADP
eurjchem-170	93	7	msn	msn	NOUN
eurjchem-170	93	8	system	system	NOUN
eurjchem-170	93	9	were	be	AUX
eurjchem-170	93	10	:	:	PUNCT
eurjchem-170	93	11	capillary	capillary	ADJ
eurjchem-170	93	12	temperature	temperature	NOUN
eurjchem-170	93	13	,	,	PUNCT
eurjchem-170	93	14	300	300	NUM
eurjchem-170	93	15	°	°	NOUN
eurjchem-170	93	16	c	c	NOUN
eurjchem-170	93	17	;	;	PUNCT
eurjchem-170	93	18	capillary	capillary	ADJ
eurjchem-170	93	19	voltage	voltage	NOUN
eurjchem-170	93	20	,	,	PUNCT
eurjchem-170	93	21	30	30	NUM
eurjchem-170	93	22	v	v	NOUN
eurjchem-170	93	23	;	;	PUNCT
eurjchem-170	93	24	tube	tube	NOUN
eurjchem-170	93	25	lens	len	NOUN
eurjchem-170	93	26	,	,	PUNCT
eurjchem-170	93	27	90	90	NUM
eurjchem-170	93	28	v	v	NOUN
eurjchem-170	93	29	;	;	PUNCT
eurjchem-170	93	30	spray	spray	NOUN
eurjchem-170	93	31	voltage	voltage	NOUN
eurjchem-170	93	32	,	,	PUNCT
eurjchem-170	93	33	5.0	5.0	NUM
eurjchem-170	93	34	kv	kv	NOUN
eurjchem-170	93	35	,	,	PUNCT
eurjchem-170	93	36	and	and	CCONJ
eurjchem-170	93	37	sheath	sheath	NOUN
eurjchem-170	93	38	gas	gas	NOUN
eurjchem-170	93	39	flow	flow	NOUN
eurjchem-170	93	40	rate	rate	NOUN
eurjchem-170	93	41	,	,	PUNCT
eurjchem-170	93	42	30	30	NUM
eurjchem-170	93	43	arb	arb	NOUN
eurjchem-170	93	44	.	.	PROPN
eurjchem-170	93	45	3.3	3.3	NUM
eurjchem-170	93	46	.	.	PUNCT
eurjchem-170	94	1	mass	mass	ADJ
eurjchem-170	94	2	fragmentation	fragmentation	NOUN
eurjchem-170	94	3	of	of	ADP
eurjchem-170	94	4	the	the	DET
eurjchem-170	94	5	drug	drug	NOUN
eurjchem-170	94	6	ms	ms	PROPN
eurjchem-170	94	7	/	/	SYM
eurjchem-170	94	8	tof	tof	PROPN
eurjchem-170	94	9	spectrum	spectrum	NOUN
eurjchem-170	94	10	of	of	ADP
eurjchem-170	94	11	the	the	DET
eurjchem-170	94	12	drug	drug	NOUN
eurjchem-170	94	13	showed	show	VERB
eurjchem-170	94	14	sixteen	sixteen	NUM
eurjchem-170	94	15	fragments	fragment	NOUN
eurjchem-170	94	16	in	in	ADP
eurjchem-170	94	17	total	total	ADJ
eurjchem-170	94	18	(	(	PUNCT
eurjchem-170	94	19	figure	figure	NOUN
eurjchem-170	94	20	2a	2a	NUM
eurjchem-170	94	21	;	;	PUNCT
eurjchem-170	94	22	labelled	label	VERB
eurjchem-170	94	23	a	a	PRON
eurjchem-170	94	24	to	to	ADP
eurjchem-170	94	25	p	p	NUM
eurjchem-170	94	26	)	)	PUNCT
eurjchem-170	94	27	.	.	PUNCT
eurjchem-170	95	1	their	their	PRON
eurjchem-170	95	2	accurate	accurate	ADJ
eurjchem-170	95	3	mass	mass	NOUN
eurjchem-170	95	4	,	,	PUNCT
eurjchem-170	95	5	possible	possible	ADJ
eurjchem-170	95	6	molecular	molecular	ADJ
eurjchem-170	95	7	formula	formula	NOUN
eurjchem-170	95	8	,	,	PUNCT
eurjchem-170	95	9	exact	exact	ADJ
eurjchem-170	95	10	theoretical	theoretical	ADJ
eurjchem-170	95	11	mass	mass	NOUN
eurjchem-170	95	12	,	,	PUNCT
eurjchem-170	95	13	error	error	NOUN
eurjchem-170	95	14	in	in	ADP
eurjchem-170	95	15	mmu	mmu	PROPN
eurjchem-170	95	16	,	,	PUNCT
eurjchem-170	95	17	ring	ring	NOUN
eurjchem-170	95	18	plus	plus	CCONJ
eurjchem-170	95	19	double	double	ADJ
eurjchem-170	95	20	bond	bond	NOUN
eurjchem-170	95	21	(	(	PUNCT
eurjchem-170	95	22	rdb	rdb	NOUN
eurjchem-170	95	23	)	)	PUNCT
eurjchem-170	95	24	value	value	NOUN
eurjchem-170	95	25	and	and	CCONJ
eurjchem-170	95	26	the	the	DET
eurjchem-170	95	27	number	number	NOUN
eurjchem-170	95	28	of	of	ADP
eurjchem-170	95	29	labile	labile	ADJ
eurjchem-170	95	30	hydrogen(s	hydrogen(s	NOUN
eurjchem-170	95	31	)	)	PUNCT
eurjchem-170	95	32	determined	determine	VERB
eurjchem-170	95	33	from	from	ADP
eurjchem-170	95	34	h	h	NOUN
eurjchem-170	95	35	/	/	SYM
eurjchem-170	95	36	d	d	NOUN
eurjchem-170	95	37	exchange	exchange	NOUN
eurjchem-170	95	38	studies	study	NOUN
eurjchem-170	95	39	are	be	AUX
eurjchem-170	95	40	given	give	VERB
eurjchem-170	95	41	in	in	ADP
eurjchem-170	95	42	table	table	NOUN
eurjchem-170	95	43	1	1	NUM
eurjchem-170	95	44	.	.	PUNCT
eurjchem-170	96	1	the	the	DET
eurjchem-170	96	2	msn	msn	PROPN
eurjchem-170	96	3	data	datum	NOUN
eurjchem-170	96	4	are	be	AUX
eurjchem-170	96	5	listed	list	VERB
eurjchem-170	96	6	in	in	ADP
eurjchem-170	96	7	table	table	NOUN
eurjchem-170	96	8	2	2	NUM
eurjchem-170	96	9	.	.	PUNCT
eurjchem-170	97	1	these	these	PRON
eurjchem-170	97	2	were	be	AUX
eurjchem-170	97	3	employed	employ	VERB
eurjchem-170	97	4	to	to	PART
eurjchem-170	97	5	establish	establish	VERB
eurjchem-170	97	6	fragmentation	fragmentation	NOUN
eurjchem-170	97	7	pathway	pathway	NOUN
eurjchem-170	97	8	for	for	ADP
eurjchem-170	97	9	the	the	DET
eurjchem-170	97	10	drug	drug	NOUN
eurjchem-170	97	11	,	,	PUNCT
eurjchem-170	97	12	as	as	SCONJ
eurjchem-170	97	13	shown	show	VERB
eurjchem-170	97	14	in	in	ADP
eurjchem-170	97	15	figure	figure	NOUN
eurjchem-170	97	16	3	3	NUM
eurjchem-170	97	17	.	.	PUNCT
eurjchem-170	97	18	based	base	VERB
eurjchem-170	97	19	on	on	ADP
eurjchem-170	97	20	the	the	DET
eurjchem-170	97	21	possibilities	possibility	NOUN
eurjchem-170	97	22	of	of	ADP
eurjchem-170	97	23	protonation	protonation	NOUN
eurjchem-170	97	24	in	in	ADP
eurjchem-170	97	25	the	the	DET
eurjchem-170	97	26	drug	drug	NOUN
eurjchem-170	97	27	structure	structure	NOUN
eurjchem-170	97	28	,	,	PUNCT
eurjchem-170	97	29	four	four	NUM
eurjchem-170	97	30	routes	route	NOUN
eurjchem-170	97	31	were	be	AUX
eurjchem-170	97	32	assigned	assign	VERB
eurjchem-170	97	33	for	for	ADP
eurjchem-170	97	34	its	its	PRON
eurjchem-170	97	35	fragmentation	fragmentation	NOUN
eurjchem-170	97	36	.	.	PUNCT
eurjchem-170	98	1	the	the	DET
eurjchem-170	98	2	first	first	ADJ
eurjchem-170	98	3	two	two	NUM
eurjchem-170	98	4	were	be	AUX
eurjchem-170	98	5	inter‐related	inter‐relate	VERB
eurjchem-170	98	6	,	,	PUNCT
eurjchem-170	98	7	and	and	CCONJ
eurjchem-170	98	8	proceeded	proceed	VERB
eurjchem-170	98	9	with	with	ADP
eurjchem-170	98	10	subsequent	subsequent	ADJ
eurjchem-170	98	11	losses	loss	NOUN
eurjchem-170	98	12	of	of	ADP
eurjchem-170	98	13	h2o	h2o	PROPN
eurjchem-170	98	14	or	or	CCONJ
eurjchem-170	98	15	co	co	VERB
eurjchem-170	98	16	to	to	PART
eurjchem-170	98	17	generate	generate	VERB
eurjchem-170	98	18	fragments	fragment	NOUN
eurjchem-170	98	19	of	of	ADP
eurjchem-170	98	20	m	m	NOUN
eurjchem-170	98	21	/	/	SYM
eurjchem-170	98	22	z	z	PROPN
eurjchem-170	98	23	407	407	NUM
eurjchem-170	98	24	,	,	PUNCT
eurjchem-170	98	25	m	m	NOUN
eurjchem-170	98	26	/	/	SYM
eurjchem-170	98	27	z	z	PROPN
eurjchem-170	98	28	389	389	NUM
eurjchem-170	98	29	,	,	PUNCT
eurjchem-170	98	30	m	m	NOUN
eurjchem-170	98	31	/	/	SYM
eurjchem-170	98	32	z	z	PROPN
eurjchem-170	98	33	379	379	NUM
eurjchem-170	98	34	and	and	CCONJ
eurjchem-170	98	35	m	m	PROPN
eurjchem-170	98	36	/	/	SYM
eurjchem-170	98	37	z	z	PROPN
eurjchem-170	98	38	361	361	NUM
eurjchem-170	98	39	.	.	PUNCT
eurjchem-170	99	1	the	the	DET
eurjchem-170	99	2	third	third	ADJ
eurjchem-170	99	3	and	and	CCONJ
eurjchem-170	99	4	major	major	ADJ
eurjchem-170	99	5	route	route	NOUN
eurjchem-170	99	6	was	be	AUX
eurjchem-170	99	7	initiated	initiate	VERB
eurjchem-170	99	8	by	by	ADP
eurjchem-170	99	9	the	the	DET
eurjchem-170	99	10	loss	loss	NOUN
eurjchem-170	99	11	of	of	ADP
eurjchem-170	99	12	thiophene	thiophene	NOUN
eurjchem-170	99	13	,	,	PUNCT
eurjchem-170	99	14	yielding	yield	VERB
eurjchem-170	99	15	a	a	DET
eurjchem-170	99	16	fragment	fragment	NOUN
eurjchem-170	99	17	of	of	ADP
eurjchem-170	99	18	m	m	PROPN
eurjchem-170	99	19	/	/	SYM
eurjchem-170	99	20	z	z	PROPN
eurjchem-170	99	21	341	341	NUM
eurjchem-170	99	22	that	that	PRON
eurjchem-170	99	23	was	be	AUX
eurjchem-170	99	24	further	far	ADV
eurjchem-170	99	25	reduced	reduce	VERB
eurjchem-170	99	26	to	to	ADP
eurjchem-170	99	27	ions	ion	NOUN
eurjchem-170	99	28	of	of	ADP
eurjchem-170	99	29	m	m	NOUN
eurjchem-170	99	30	/	/	SYM
eurjchem-170	99	31	z	z	PROPN
eurjchem-170	99	32	297	297	NUM
eurjchem-170	99	33	and	and	CCONJ
eurjchem-170	99	34	m	m	PROPN
eurjchem-170	99	35	/	/	SYM
eurjchem-170	99	36	z	z	PROPN
eurjchem-170	99	37	207	207	NUM
eurjchem-170	99	38	through	through	ADP
eurjchem-170	99	39	neutral	neutral	ADJ
eurjchem-170	99	40	loss	loss	NOUN
eurjchem-170	99	41	of	of	ADP
eurjchem-170	99	42	co2	co2	NOUN
eurjchem-170	99	43	and	and	CCONJ
eurjchem-170	99	44	c8h6o2	c8h6o2	NOUN
eurjchem-170	99	45	,	,	PUNCT
eurjchem-170	99	46	respectively	respectively	ADV
eurjchem-170	99	47	.	.	PUNCT
eurjchem-170	100	1	both	both	DET
eurjchem-170	100	2	these	these	DET
eurjchem-170	100	3	ions	ion	NOUN
eurjchem-170	100	4	further	far	ADV
eurjchem-170	100	5	produced	produce	VERB
eurjchem-170	100	6	a	a	DET
eurjchem-170	100	7	fragment	fragment	NOUN
eurjchem-170	100	8	of	of	ADP
eurjchem-170	100	9	m	m	PROPN
eurjchem-170	100	10	/	/	SYM
eurjchem-170	100	11	z	z	PROPN
eurjchem-170	100	12	163	163	NUM
eurjchem-170	100	13	by	by	ADP
eurjchem-170	100	14	respective	respective	ADJ
eurjchem-170	100	15	neutral	neutral	ADJ
eurjchem-170	100	16	losses	loss	NOUN
eurjchem-170	100	17	of	of	ADP
eurjchem-170	100	18	c8h6o2	c8h6o2	NOUN
eurjchem-170	100	19	and	and	CCONJ
eurjchem-170	100	20	co2	co2	NOUN
eurjchem-170	100	21	.	.	PUNCT
eurjchem-170	101	1	the	the	DET
eurjchem-170	101	2	fourth	fourth	ADJ
eurjchem-170	101	3	route	route	NOUN
eurjchem-170	101	4	,	,	PUNCT
eurjchem-170	101	5	which	which	PRON
eurjchem-170	101	6	involved	involve	VERB
eurjchem-170	101	7	protonation	protonation	NOUN
eurjchem-170	101	8	of	of	ADP
eurjchem-170	101	9	imidazole	imidazole	NOUN
eurjchem-170	101	10	ring	ring	NOUN
eurjchem-170	101	11	,	,	PUNCT
eurjchem-170	101	12	cleaved	cleave	VERB
eurjchem-170	101	13	the	the	DET
eurjchem-170	101	14	drug	drug	NOUN
eurjchem-170	101	15	into	into	ADP
eurjchem-170	101	16	two	two	NUM
eurjchem-170	101	17	major	major	ADJ
eurjchem-170	101	18	fragments	fragment	NOUN
eurjchem-170	101	19	of	of	ADP
eurjchem-170	101	20	m	m	PROPN
eurjchem-170	101	21	/	/	SYM
eurjchem-170	101	22	z	z	PROPN
eurjchem-170	101	23	291	291	NUM
eurjchem-170	101	24	and	and	CCONJ
eurjchem-170	101	25	m	m	PROPN
eurjchem-170	101	26	/	/	SYM
eurjchem-170	101	27	z	z	PROPN
eurjchem-170	101	28	135	135	NUM
eurjchem-170	101	29	and	and	CCONJ
eurjchem-170	101	30	a	a	DET
eurjchem-170	101	31	minor	minor	NOUN
eurjchem-170	101	32	of	of	ADP
eurjchem-170	101	33	m	m	PROPN
eurjchem-170	101	34	/	/	SYM
eurjchem-170	101	35	z	z	PROPN
eurjchem-170	101	36	290	290	NUM
eurjchem-170	101	37	.	.	PUNCT
eurjchem-170	102	1	the	the	DET
eurjchem-170	102	2	ion	ion	NOUN
eurjchem-170	102	3	of	of	ADP
eurjchem-170	102	4	m	m	PROPN
eurjchem-170	102	5	/	/	SYM
eurjchem-170	102	6	z	z	PROPN
eurjchem-170	102	7	291	291	NUM
eurjchem-170	102	8	first	first	ADV
eurjchem-170	102	9	lost	lose	VERB
eurjchem-170	102	10	h2o	h2o	NOUN
eurjchem-170	102	11	and	and	CCONJ
eurjchem-170	102	12	then	then	ADV
eurjchem-170	102	13	co	co	VERB
eurjchem-170	102	14	to	to	PART
eurjchem-170	102	15	yield	yield	VERB
eurjchem-170	102	16	daughters	daughter	NOUN
eurjchem-170	102	17	of	of	ADP
eurjchem-170	102	18	m	m	PROPN
eurjchem-170	102	19	/	/	SYM
eurjchem-170	102	20	z	z	PROPN
eurjchem-170	102	21	273	273	NUM
eurjchem-170	102	22	and	and	CCONJ
eurjchem-170	102	23	m	m	PROPN
eurjchem-170	102	24	/	/	SYM
eurjchem-170	102	25	z	z	PROPN
eurjchem-170	102	26	245	245	NUM
eurjchem-170	102	27	,	,	PUNCT
eurjchem-170	102	28	respectively	respectively	ADV
eurjchem-170	102	29	.	.	PUNCT
eurjchem-170	103	1	the	the	DET
eurjchem-170	103	2	pathway	pathway	NOUN
eurjchem-170	103	3	m	m	PROPN
eurjchem-170	103	4	/	/	SYM
eurjchem-170	103	5	z	z	PROPN
eurjchem-170	103	6	290	290	NUM
eurjchem-170	103	7			NOUN
eurjchem-170	103	8	m	m	ADJ
eurjchem-170	103	9	/	/	SYM
eurjchem-170	103	10	z	z	PROPN
eurjchem-170	103	11	272	272	NUM
eurjchem-170	103	12			NOUN
eurjchem-170	103	13	m	m	PROPN
eurjchem-170	103	14	/	/	SYM
eurjchem-170	103	15	z	z	PROPN
eurjchem-170	103	16	244	244	NUM
eurjchem-170	103	17	involved	involve	VERB
eurjchem-170	103	18	loss	loss	NOUN
eurjchem-170	103	19	of	of	ADP
eurjchem-170	103	20	the	the	DET
eurjchem-170	103	21	substituted	substitute	VERB
eurjchem-170	103	22	phenyl	phenyl	NOUN
eurjchem-170	103	23	moiety	moiety	NOUN
eurjchem-170	103	24	without	without	ADP
eurjchem-170	103	25	hydrogen	hydrogen	NOUN
eurjchem-170	103	26	transfer	transfer	NOUN
eurjchem-170	103	27	to	to	ADP
eurjchem-170	103	28	the	the	DET
eurjchem-170	103	29	imidazole	imidazole	NOUN
eurjchem-170	103	30	ring	ring	NOUN
eurjchem-170	103	31	,	,	PUNCT
eurjchem-170	103	32	which	which	PRON
eurjchem-170	103	33	could	could	AUX
eurjchem-170	103	34	only	only	ADV
eurjchem-170	103	35	be	be	AUX
eurjchem-170	103	36	justified	justify	VERB
eurjchem-170	103	37	through	through	ADP
eurjchem-170	103	38	the	the	DET
eurjchem-170	103	39	formation	formation	NOUN
eurjchem-170	103	40	of	of	ADP
eurjchem-170	103	41	radical	radical	ADJ
eurjchem-170	103	42	cations	cation	NOUN
eurjchem-170	103	43	.	.	PUNCT
eurjchem-170	104	1	3.4	3.4	NUM
eurjchem-170	104	2	.	.	PUNCT
eurjchem-170	104	3	lc‐ms	lc‐ms	AUX
eurjchem-170	104	4	/	/	SYM
eurjchem-170	104	5	tof	tof	PROPN
eurjchem-170	104	6	and	and	CCONJ
eurjchem-170	104	7	on‐line	on‐line	PROPN
eurjchem-170	104	8	h	h	NOUN
eurjchem-170	104	9	/	/	SYM
eurjchem-170	104	10	d	d	PROPN
eurjchem-170	104	11	exchange	exchange	NOUN
eurjchem-170	104	12	studies	study	NOUN
eurjchem-170	104	13	lc‐ms	lc‐ms	AUX
eurjchem-170	104	14	/	/	SYM
eurjchem-170	105	1	tof	tof	PRON
eurjchem-170	105	2	studies	study	NOUN
eurjchem-170	105	3	on	on	ADP
eurjchem-170	105	4	the	the	DET
eurjchem-170	105	5	drug	drug	NOUN
eurjchem-170	105	6	(	(	PUNCT
eurjchem-170	105	7	figure	figure	NOUN
eurjchem-170	105	8	2a	2a	NUM
eurjchem-170	105	9	)	)	PUNCT
eurjchem-170	105	10	and	and	CCONJ
eurjchem-170	105	11	its	its	PRON
eurjchem-170	105	12	product	product	NOUN
eurjchem-170	105	13	(	(	PUNCT
eurjchem-170	105	14	figure	figure	NOUN
eurjchem-170	105	15	2b	2b	NOUN
eurjchem-170	105	16	)	)	PUNCT
eurjchem-170	105	17	showed	show	VERB
eurjchem-170	105	18	the	the	DET
eurjchem-170	105	19	latter	latter	ADJ
eurjchem-170	105	20	to	to	PART
eurjchem-170	105	21	have	have	VERB
eurjchem-170	105	22	the	the	DET
eurjchem-170	105	23	same	same	ADJ
eurjchem-170	105	24	mass	mass	NOUN
eurjchem-170	105	25	profile	profile	NOUN
eurjchem-170	105	26	as	as	ADP
eurjchem-170	105	27	that	that	PRON
eurjchem-170	105	28	of	of	ADP
eurjchem-170	105	29	the	the	DET
eurjchem-170	105	30	drug	drug	NOUN
eurjchem-170	105	31	.	.	PUNCT
eurjchem-170	106	1	the	the	DET
eurjchem-170	106	2	calculated	calculate	VERB
eurjchem-170	106	3	chemical	chemical	NOUN
eurjchem-170	106	4	formula	formula	NOUN
eurjchem-170	106	5	for	for	ADP
eurjchem-170	106	6	each	each	DET
eurjchem-170	106	7	fragment	fragment	NOUN
eurjchem-170	106	8	(	(	PUNCT
eurjchem-170	106	9	table	table	NOUN
eurjchem-170	106	10	1	1	NUM
eurjchem-170	106	11	)	)	PUNCT
eurjchem-170	106	12	was	be	AUX
eurjchem-170	106	13	also	also	ADV
eurjchem-170	106	14	same	same	ADJ
eurjchem-170	106	15	for	for	ADP
eurjchem-170	106	16	the	the	DET
eurjchem-170	106	17	both	both	NOUN
eurjchem-170	106	18	.	.	PUNCT
eurjchem-170	107	1	even	even	ADV
eurjchem-170	107	2	on‐line	on‐line	PROPN
eurjchem-170	107	3	h	h	NOUN
eurjchem-170	107	4	/	/	SYM
eurjchem-170	107	5	d	d	NOUN
eurjchem-170	107	6	exchange	exchange	NOUN
eurjchem-170	107	7	studies	study	NOUN
eurjchem-170	107	8	showed	show	VERB
eurjchem-170	107	9	the	the	DET
eurjchem-170	107	10	same	same	ADJ
eurjchem-170	107	11	molecular	molecular	ADJ
eurjchem-170	107	12	mass	mass	NOUN
eurjchem-170	107	13	of	of	ADP
eurjchem-170	107	14	m	m	PROPN
eurjchem-170	107	15	/	/	SYM
eurjchem-170	107	16	z	z	PROPN
eurjchem-170	107	17	428	428	NUM
eurjchem-170	107	18	for	for	ADP
eurjchem-170	107	19	the	the	DET
eurjchem-170	107	20	drug	drug	NOUN
eurjchem-170	107	21	and	and	CCONJ
eurjchem-170	107	22	the	the	DET
eurjchem-170	107	23	product	product	NOUN
eurjchem-170	107	24	,	,	PUNCT
eurjchem-170	107	25	indicating	indicate	VERB
eurjchem-170	107	26	same	same	ADJ
eurjchem-170	107	27	number	number	NOUN
eurjchem-170	107	28	of	of	ADP
eurjchem-170	107	29	the	the	DET
eurjchem-170	107	30	labile	labile	ADJ
eurjchem-170	107	31	hydrogens	hydrogen	NOUN
eurjchem-170	107	32	.	.	PUNCT
eurjchem-170	108	1	the	the	DET
eurjchem-170	108	2	only	only	ADJ
eurjchem-170	108	3	difference	difference	NOUN
eurjchem-170	108	4	was	be	AUX
eurjchem-170	108	5	in	in	ADP
eurjchem-170	108	6	relative	relative	ADJ
eurjchem-170	108	7	fragment	fragment	NOUN
eurjchem-170	108	8	ion	ion	NOUN
eurjchem-170	108	9	intensities	intensity	NOUN
eurjchem-170	108	10	in	in	ADP
eurjchem-170	108	11	ms	ms	PROPN
eurjchem-170	108	12	/	/	SYM
eurjchem-170	108	13	tof	tof	PROPN
eurjchem-170	108	14	spectra	spectra	NOUN
eurjchem-170	108	15	(	(	PUNCT
eurjchem-170	108	16	figure	figure	NOUN
eurjchem-170	108	17	2	2	NUM
eurjchem-170	108	18	)	)	PUNCT
eurjchem-170	108	19	,	,	PUNCT
eurjchem-170	108	20	which	which	PRON
eurjchem-170	108	21	was	be	AUX
eurjchem-170	108	22	seen	see	VERB
eurjchem-170	108	23	even	even	ADV
eurjchem-170	108	24	on	on	ADP
eurjchem-170	108	25	repeated	repeat	VERB
eurjchem-170	108	26	injections	injection	NOUN
eurjchem-170	108	27	.	.	PUNCT
eurjchem-170	109	1	while	while	SCONJ
eurjchem-170	109	2	the	the	DET
eurjchem-170	109	3	ion	ion	NOUN
eurjchem-170	109	4	of	of	ADP
eurjchem-170	109	5	m	m	PROPN
eurjchem-170	109	6	/	/	SYM
eurjchem-170	109	7	z	z	PROPN
eurjchem-170	109	8	207	207	NUM
eurjchem-170	109	9	(	(	PUNCT
eurjchem-170	109	10	53.1	53.1	NUM
eurjchem-170	109	11	%	%	NOUN
eurjchem-170	109	12	)	)	PUNCT
eurjchem-170	109	13	was	be	AUX
eurjchem-170	109	14	most	most	ADV
eurjchem-170	109	15	prominent	prominent	ADJ
eurjchem-170	109	16	in	in	ADP
eurjchem-170	109	17	case	case	NOUN
eurjchem-170	109	18	of	of	ADP
eurjchem-170	109	19	the	the	DET
eurjchem-170	109	20	drug	drug	NOUN
eurjchem-170	109	21	,	,	PUNCT
eurjchem-170	109	22	the	the	DET
eurjchem-170	109	23	same	same	ADJ
eurjchem-170	109	24	was	be	AUX
eurjchem-170	109	25	very	very	ADV
eurjchem-170	109	26	low	low	ADV
eurjchem-170	109	27	abundant	abundant	ADJ
eurjchem-170	109	28	(	(	PUNCT
eurjchem-170	109	29	3.1	3.1	NUM
eurjchem-170	109	30	%	%	NOUN
eurjchem-170	109	31	)	)	PUNCT
eurjchem-170	109	32	in	in	ADP
eurjchem-170	109	33	the	the	DET
eurjchem-170	109	34	degradation	degradation	NOUN
eurjchem-170	109	35	product	product	NOUN
eurjchem-170	109	36	.	.	PUNCT
eurjchem-170	110	1	a	a	DET
eurjchem-170	110	2	similar	similar	ADJ
eurjchem-170	110	3	situation	situation	NOUN
eurjchem-170	110	4	existed	exist	VERB
eurjchem-170	110	5	for	for	ADP
eurjchem-170	110	6	the	the	DET
eurjchem-170	110	7	fragment	fragment	NOUN
eurjchem-170	110	8	of	of	ADP
eurjchem-170	110	9	m	m	PROPN
eurjchem-170	110	10	/	/	SYM
eurjchem-170	110	11	z	z	PROPN
eurjchem-170	110	12	341	341	NUM
eurjchem-170	110	13	.	.	PUNCT
eurjchem-170	111	1	conversely	conversely	ADV
eurjchem-170	111	2	,	,	PUNCT
eurjchem-170	111	3	abundance	abundance	NOUN
eurjchem-170	111	4	of	of	ADP
eurjchem-170	111	5	the	the	DET
eurjchem-170	111	6	fragment	fragment	NOUN
eurjchem-170	111	7	of	of	ADP
eurjchem-170	111	8	m	m	PROPN
eurjchem-170	111	9	/	/	SYM
eurjchem-170	111	10	z	z	PROPN
eurjchem-170	111	11	273	273	NUM
eurjchem-170	111	12	was	be	AUX
eurjchem-170	111	13	higher	high	ADJ
eurjchem-170	111	14	in	in	ADP
eurjchem-170	111	15	the	the	DET
eurjchem-170	111	16	product	product	NOUN
eurjchem-170	111	17	(	(	PUNCT
eurjchem-170	111	18	43.5	43.5	NUM
eurjchem-170	111	19	%	%	NOUN
eurjchem-170	111	20	)	)	PUNCT
eurjchem-170	111	21	than	than	ADP
eurjchem-170	111	22	the	the	DET
eurjchem-170	111	23	corresponding	corresponding	ADJ
eurjchem-170	111	24	ion	ion	NOUN
eurjchem-170	111	25	in	in	ADP
eurjchem-170	111	26	case	case	NOUN
eurjchem-170	111	27	of	of	ADP
eurjchem-170	111	28	the	the	DET
eurjchem-170	111	29	drug	drug	NOUN
eurjchem-170	111	30	(	(	PUNCT
eurjchem-170	111	31	6.8	6.8	NUM
eurjchem-170	111	32	%	%	NOUN
eurjchem-170	111	33	)	)	PUNCT
eurjchem-170	111	34	.	.	PUNCT
eurjchem-170	112	1	(	(	PUNCT
eurjchem-170	112	2	a	a	X
eurjchem-170	112	3	)	)	PUNCT
eurjchem-170	112	4	(	(	PUNCT
eurjchem-170	112	5	b	b	X
eurjchem-170	112	6	)	)	PUNCT
eurjchem-170	112	7	figure	figure	NOUN
eurjchem-170	112	8	2	2	NUM
eurjchem-170	112	9	.	.	PUNCT
eurjchem-170	112	10	lc‐ms	lc‐ms	AUX
eurjchem-170	112	11	/	/	SYM
eurjchem-170	112	12	tof	tof	PROPN
eurjchem-170	112	13	spectrum	spectrum	NOUN
eurjchem-170	112	14	of	of	ADP
eurjchem-170	112	15	the	the	DET
eurjchem-170	112	16	drug	drug	NOUN
eurjchem-170	112	17	(	(	PUNCT
eurjchem-170	112	18	a	a	NOUN
eurjchem-170	112	19	)	)	PUNCT
eurjchem-170	112	20	and	and	CCONJ
eurjchem-170	112	21	the	the	DET
eurjchem-170	112	22	product	product	NOUN
eurjchem-170	112	23	(	(	PUNCT
eurjchem-170	112	24	b	b	NOUN
eurjchem-170	112	25	)	)	PUNCT
eurjchem-170	112	26	;	;	PUNCT
eurjchem-170	112	27	the	the	DET
eurjchem-170	112	28	labels	label	NOUN
eurjchem-170	112	29	a‐p	a‐p	ADV
eurjchem-170	112	30	are	be	AUX
eurjchem-170	112	31	for	for	ADP
eurjchem-170	112	32	different	different	ADJ
eurjchem-170	112	33	fragments	fragment	NOUN
eurjchem-170	112	34	of	of	ADP
eurjchem-170	112	35	the	the	DET
eurjchem-170	112	36	drug	drug	NOUN
eurjchem-170	112	37	.	.	PUNCT
eurjchem-170	113	1	the	the	DET
eurjchem-170	113	2	same	same	ADJ
eurjchem-170	113	3	apply	apply	VERB
eurjchem-170	113	4	even	even	ADV
eurjchem-170	113	5	to	to	ADP
eurjchem-170	113	6	the	the	DET
eurjchem-170	113	7	fragments	fragment	NOUN
eurjchem-170	113	8	for	for	ADP
eurjchem-170	113	9	the	the	DET
eurjchem-170	113	10	product	product	NOUN
eurjchem-170	113	11	in	in	ADP
eurjchem-170	113	12	lower	low	ADJ
eurjchem-170	113	13	figure	figure	NOUN
eurjchem-170	113	14	b.	b.	NOUN
eurjchem-170	113	15	3.5	3.5	NUM
eurjchem-170	113	16	.	.	PUNCT
eurjchem-170	114	1	lc‐nmr	lc‐nmr	PROPN
eurjchem-170	114	2	study	study	NOUN
eurjchem-170	114	3	1h	1h	NUM
eurjchem-170	114	4	lc‐nmr	lc‐nmr	PROPN
eurjchem-170	114	5	spectra	spectra	NOUN
eurjchem-170	114	6	of	of	ADP
eurjchem-170	114	7	the	the	DET
eurjchem-170	114	8	drug	drug	NOUN
eurjchem-170	114	9	and	and	CCONJ
eurjchem-170	114	10	the	the	DET
eurjchem-170	114	11	product	product	NOUN
eurjchem-170	114	12	are	be	AUX
eurjchem-170	114	13	shown	show	VERB
eurjchem-170	114	14	in	in	ADP
eurjchem-170	114	15	figure	figure	NOUN
eurjchem-170	114	16	4	4	NUM
eurjchem-170	114	17	.	.	PUNCT
eurjchem-170	115	1	the	the	DET
eurjchem-170	115	2	corresponding	correspond	VERB
eurjchem-170	115	3	1h	1h	NUM
eurjchem-170	115	4	peak	peak	NOUN
eurjchem-170	115	5	assignments	assignment	NOUN
eurjchem-170	115	6	along	along	ADP
eurjchem-170	115	7	with	with	ADP
eurjchem-170	115	8	multiplicity	multiplicity	NOUN
eurjchem-170	115	9	and	and	CCONJ
eurjchem-170	115	10	coupling	coupling	NOUN
eurjchem-170	115	11	constants	constant	NOUN
eurjchem-170	115	12	,	,	PUNCT
eurjchem-170	115	13	and	and	CCONJ
eurjchem-170	115	14	cosy	cosy	NOUN
eurjchem-170	115	15	correlations	correlation	NOUN
eurjchem-170	115	16	are	be	AUX
eurjchem-170	115	17	given	give	VERB
eurjchem-170	115	18	in	in	ADP
eurjchem-170	115	19	table	table	NOUN
eurjchem-170	115	20	3	3	NUM
eurjchem-170	115	21	.	.	PUNCT
eurjchem-170	116	1	the	the	DET
eurjchem-170	116	2	prominent	prominent	ADJ
eurjchem-170	116	3	peaks	peak	NOUN
eurjchem-170	116	4	for	for	ADP
eurjchem-170	116	5	the	the	DET
eurjchem-170	116	6	drug	drug	NOUN
eurjchem-170	116	7	included	include	VERB
eurjchem-170	116	8	:	:	PUNCT
eurjchem-170	116	9	(	(	PUNCT
eurjchem-170	116	10	i	i	NOUN
eurjchem-170	116	11	)	)	PUNCT
eurjchem-170	116	12	two	two	NUM
eurjchem-170	116	13	doublets	doublet	NOUN
eurjchem-170	116	14	at	at	ADP
eurjchem-170	116	15	δ	δ	PROPN
eurjchem-170	116	16	7.95	7.95	NUM
eurjchem-170	116	17	and	and	CCONJ
eurjchem-170	116	18	δ	δ	PROPN
eurjchem-170	116	19	7.16	7.16	NUM
eurjchem-170	116	20	ppm	ppm	NOUN
eurjchem-170	116	21	arising	arise	VERB
eurjchem-170	116	22	due	due	ADP
eurjchem-170	116	23	to	to	ADP
eurjchem-170	116	24	two	two	NUM
eurjchem-170	116	25	aromatic	aromatic	ADJ
eurjchem-170	116	26	resonances	resonance	NOUN
eurjchem-170	116	27	corresponding	correspond	VERB
eurjchem-170	116	28	to	to	ADP
eurjchem-170	116	29	the	the	DET
eurjchem-170	116	30	positions	position	NOUN
eurjchem-170	116	31	h‐9,11	h‐9,11	NOUN
eurjchem-170	116	32	and	and	CCONJ
eurjchem-170	116	33	h‐8,12	h‐8,12	PROPN
eurjchem-170	116	34	,	,	PUNCT
eurjchem-170	116	35	respectively	respectively	ADV
eurjchem-170	116	36	;	;	PUNCT
eurjchem-170	116	37	(	(	PUNCT
eurjchem-170	116	38	ii	ii	NOUN
eurjchem-170	116	39	)	)	PUNCT
eurjchem-170	116	40	two	two	NUM
eurjchem-170	116	41	singlets	singlet	NOUN
eurjchem-170	116	42	arising	arise	VERB
eurjchem-170	116	43	from	from	ADP
eurjchem-170	116	44	h‐5	h‐5	PROPN
eurjchem-170	116	45	and	and	CCONJ
eurjchem-170	116	46	h‐13	h‐13	ADJ
eurjchem-170	116	47	at	at	ADP
eurjchem-170	116	48	δ	δ	PROPN
eurjchem-170	116	49	7.58	7.58	NUM
eurjchem-170	116	50	and	and	CCONJ
eurjchem-170	116	51	δ	δ	PROPN
eurjchem-170	116	52	7.35	7.35	NUM
eurjchem-170	116	53	ppm	ppm	NOUN
eurjchem-170	116	54	,	,	PUNCT
eurjchem-170	116	55	respectively	respectively	ADV
eurjchem-170	116	56	;	;	PUNCT
eurjchem-170	116	57	(	(	PUNCT
eurjchem-170	116	58	iii	iii	X
eurjchem-170	116	59	)	)	PUNCT
eurjchem-170	116	60	three	three	NUM
eurjchem-170	116	61	aromatic	aromatic	ADJ
eurjchem-170	116	62	resonances	resonance	NOUN
eurjchem-170	116	63	(	(	PUNCT
eurjchem-170	116	64	two	two	NUM
eurjchem-170	116	65	doublets	doublet	NOUN
eurjchem-170	116	66	,	,	PUNCT
eurjchem-170	116	67	one	one	NUM
eurjchem-170	116	68	multiplet	multiplet	NOUN
eurjchem-170	116	69	)	)	PUNCT
eurjchem-170	116	70	arising	arise	VERB
eurjchem-170	116	71	due	due	ADP
eurjchem-170	116	72	to	to	ADP
eurjchem-170	116	73	thiophene	thiophene	NOUN
eurjchem-170	116	74	ring	ring	NOUN
eurjchem-170	116	75	corresponding	correspond	VERB
eurjchem-170	116	76	to	to	ADP
eurjchem-170	116	77	h‐18	h‐18	PROPN
eurjchem-170	116	78	,	,	PUNCT
eurjchem-170	116	79	h‐20	h‐20	PROPN
eurjchem-170	116	80	and	and	CCONJ
eurjchem-170	116	81	h‐19	h‐19	PROPN
eurjchem-170	116	82	at	at	ADP
eurjchem-170	116	83	δ	δ	PROPN
eurjchem-170	116	84	7.22	7.22	NUM
eurjchem-170	116	85	,	,	PUNCT
eurjchem-170	116	86	δ	δ	PROPN
eurjchem-170	116	87	6.65	6.65	NUM
eurjchem-170	116	88	and	and	CCONJ
eurjchem-170	116	89	δ	δ	PROPN
eurjchem-170	116	90	6.90	6.90	NUM
eurjchem-170	116	91	ppm	ppm	NOUN
eurjchem-170	116	92	,	,	PUNCT
eurjchem-170	116	93	respectively	respectively	ADV
eurjchem-170	116	94	;	;	PUNCT
eurjchem-170	116	95	(	(	PUNCT
eurjchem-170	116	96	iv	iv	X
eurjchem-170	116	97	)	)	PUNCT
eurjchem-170	116	98	two	two	NUM
eurjchem-170	116	99	singlets	singlet	NOUN
eurjchem-170	116	100	corresponding	correspond	VERB
eurjchem-170	116	101	to	to	ADP
eurjchem-170	116	102	methylene	methylene	ADJ
eurjchem-170	116	103	protons	proton	NOUN
eurjchem-170	116	104	for	for	ADP
eurjchem-170	116	105	position	position	NOUN
eurjchem-170	116	106	h‐6	h‐6	NOUN
eurjchem-170	116	107	and	and	CCONJ
eurjchem-170	116	108	h‐15	h‐15	NOUN
eurjchem-170	116	109	at	at	ADP
eurjchem-170	116	110	δ	δ	PROPN
eurjchem-170	116	111	5.50	5.50	NUM
eurjchem-170	116	112	and	and	CCONJ
eurjchem-170	116	113	δ	δ	PROPN
eurjchem-170	116	114	3.96	3.96	NUM
eurjchem-170	116	115	ppm	ppm	NOUN
eurjchem-170	116	116	,	,	PUNCT
eurjchem-170	116	117	respectively	respectively	ADV
eurjchem-170	116	118	,	,	PUNCT
eurjchem-170	116	119	and	and	CCONJ
eurjchem-170	116	120	(	(	PUNCT
eurjchem-170	116	121	v	v	NOUN
eurjchem-170	116	122	)	)	PUNCT
eurjchem-170	116	123	two	two	NUM
eurjchem-170	116	124	triplets	triplet	NOUN
eurjchem-170	116	125	corresponding	correspond	VERB
eurjchem-170	116	126	to	to	ADP
eurjchem-170	116	127	methyl	methyl	NOUN
eurjchem-170	116	128	and	and	CCONJ
eurjchem-170	116	129	methylene	methylene	NOUN
eurjchem-170	116	130	protons	proton	NOUN
eurjchem-170	116	131	arising	arise	VERB
eurjchem-170	116	132	at	at	ADP
eurjchem-170	116	133	δ	δ	PROPN
eurjchem-170	116	134	0.78	0.78	NUM
eurjchem-170	116	135	and	and	CCONJ
eurjchem-170	116	136	δ	δ	PROPN
eurjchem-170	116	137	2.97	2.97	NUM
eurjchem-170	116	138	ppm	ppm	NOUN
eurjchem-170	116	139	for	for	ADP
eurjchem-170	116	140	h‐4	h‐4	NOUN
eurjchem-170	116	141	’	'	PUNCT
eurjchem-170	116	142	and	and	CCONJ
eurjchem-170	116	143	h‐1	h‐1	PROPN
eurjchem-170	116	144	’	'	PUNCT
eurjchem-170	116	145	,	,	PUNCT
eurjchem-170	116	146	respectively	respectively	ADV
eurjchem-170	116	147	,	,	PUNCT
eurjchem-170	116	148	and	and	CCONJ
eurjchem-170	116	149	two	two	NUM
eurjchem-170	116	150	multiplets	multiplet	NOUN
eurjchem-170	116	151	arising	arise	VERB
eurjchem-170	116	152	at	at	ADP
eurjchem-170	116	153	δ	δ	PROPN
eurjchem-170	116	154	1.26	1.26	NUM
eurjchem-170	116	155	and	and	CCONJ
eurjchem-170	116	156	δ	δ	PROPN
eurjchem-170	116	157	1.55	1.55	NUM
eurjchem-170	116	158	ppm	ppm	NOUN
eurjchem-170	116	159	(	(	PUNCT
eurjchem-170	116	160	h‐3	h‐3	NOUN
eurjchem-170	116	161	’	'	PUNCT
eurjchem-170	116	162	and	and	CCONJ
eurjchem-170	116	163	h‐2	h‐2	NOUN
eurjchem-170	116	164	’	'	PUNCT
eurjchem-170	116	165	)	)	PUNCT
eurjchem-170	116	166	representing	represent	VERB
eurjchem-170	116	167	the	the	DET
eurjchem-170	116	168	methylene	methylene	ADJ
eurjchem-170	116	169	protons	proton	NOUN
eurjchem-170	116	170	of	of	ADP
eurjchem-170	116	171	the	the	DET
eurjchem-170	116	172	butyl	butyl	NOUN
eurjchem-170	116	173	chain	chain	NOUN
eurjchem-170	116	174	.	.	PUNCT
eurjchem-170	117	1	further	further	ADJ
eurjchem-170	117	2	cosy	cosy	PROPN
eurjchem-170	117	3	data	datum	NOUN
eurjchem-170	117	4	(	(	PUNCT
eurjchem-170	117	5	table	table	NOUN
eurjchem-170	117	6	3	3	NUM
eurjchem-170	117	7	)	)	PUNCT
eurjchem-170	117	8	also	also	ADV
eurjchem-170	117	9	supported	support	VERB
eurjchem-170	117	10	the	the	DET
eurjchem-170	117	11	peak	peak	NOUN
eurjchem-170	117	12	assignments	assignment	NOUN
eurjchem-170	117	13	.	.	PUNCT
eurjchem-170	118	1	the	the	DET
eurjchem-170	118	2	1h	1h	NUM
eurjchem-170	118	3	lc‐nmr	lc‐nmr	PROPN
eurjchem-170	118	4	of	of	ADP
eurjchem-170	118	5	the	the	DET
eurjchem-170	118	6	product	product	NOUN
eurjchem-170	118	7	showed	show	VERB
eurjchem-170	118	8	only	only	ADV
eurjchem-170	118	9	one	one	NUM
eurjchem-170	118	10	major	major	ADJ
eurjchem-170	118	11	dissimilar	dissimilar	ADJ
eurjchem-170	118	12	peak	peak	NOUN
eurjchem-170	118	13	(	(	PUNCT
eurjchem-170	118	14	δ	δ	PROPN
eurjchem-170	118	15	5.57	5.57	NUM
eurjchem-170	118	16	ppm	ppm	NOUN
eurjchem-170	118	17	)	)	PUNCT
eurjchem-170	118	18	when	when	SCONJ
eurjchem-170	118	19	compared	compare	VERB
eurjchem-170	118	20	to	to	ADP
eurjchem-170	118	21	the	the	DET
eurjchem-170	118	22	drug	drug	NOUN
eurjchem-170	118	23	(	(	PUNCT
eurjchem-170	118	24	δ	δ	PROPN
eurjchem-170	118	25	7.35	7.35	NUM
eurjchem-170	118	26	ppm	ppm	NOUN
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eurjchem-170	118	28	.	.	PUNCT
eurjchem-170	119	1	other	other	ADJ
eurjchem-170	119	2	1h	1h	NUM
eurjchem-170	119	3	peaks	peak	NOUN
eurjchem-170	119	4	were	be	AUX
eurjchem-170	119	5	insignificantly	insignificantly	ADV
eurjchem-170	119	6	changed	change	VERB
eurjchem-170	119	7	,	,	PUNCT
eurjchem-170	119	8	while	while	SCONJ
eurjchem-170	119	9	cosy	cosy	ADJ
eurjchem-170	119	10	correlations	correlation	NOUN
eurjchem-170	119	11	were	be	AUX
eurjchem-170	119	12	the	the	DET
eurjchem-170	119	13	same	same	ADJ
eurjchem-170	119	14	to	to	ADP
eurjchem-170	119	15	the	the	DET
eurjchem-170	119	16	drug	drug	NOUN
eurjchem-170	119	17	(	(	PUNCT
eurjchem-170	119	18	table	table	NOUN
eurjchem-170	119	19	3	3	NUM
eurjchem-170	119	20	)	)	PUNCT
eurjchem-170	119	21	.	.	PUNCT
eurjchem-170	120	1	3.6	3.6	NUM
eurjchem-170	120	2	.	.	PUNCT
eurjchem-170	120	3	structure	structure	NOUN
eurjchem-170	120	4	elucidation	elucidation	NOUN
eurjchem-170	120	5	as	as	SCONJ
eurjchem-170	120	6	discussed	discuss	VERB
eurjchem-170	120	7	above	above	ADV
eurjchem-170	120	8	,	,	PUNCT
eurjchem-170	120	9	identical	identical	ADJ
eurjchem-170	120	10	molecular	molecular	ADJ
eurjchem-170	120	11	ion	ion	NOUN
eurjchem-170	120	12	mass	mass	NOUN
eurjchem-170	120	13	and	and	CCONJ
eurjchem-170	120	14	similar	similar	ADJ
eurjchem-170	120	15	fragmentation	fragmentation	NOUN
eurjchem-170	120	16	profile	profile	NOUN
eurjchem-170	120	17	in	in	ADP
eurjchem-170	120	18	lc‐ms	lc‐ms	PROPN
eurjchem-170	120	19	study	study	NOUN
eurjchem-170	120	20	revealed	reveal	VERB
eurjchem-170	120	21	that	that	SCONJ
eurjchem-170	120	22	the	the	DET
eurjchem-170	120	23	product	product	NOUN
eurjchem-170	120	24	was	be	AUX
eurjchem-170	120	25	an	an	DET
eurjchem-170	120	26	isomer	isomer	NOUN
eurjchem-170	120	27	of	of	ADP
eurjchem-170	120	28	the	the	DET
eurjchem-170	120	29	drug	drug	NOUN
eurjchem-170	120	30	.	.	PUNCT
eurjchem-170	121	1	this	this	PRON
eurjchem-170	121	2	was	be	AUX
eurjchem-170	121	3	verified	verify	VERB
eurjchem-170	121	4	through	through	ADP
eurjchem-170	121	5	distinguishing	distinguish	VERB
eurjchem-170	121	6	spectral	spectral	ADJ
eurjchem-170	121	7	difference	difference	NOUN
eurjchem-170	121	8	in	in	ADP
eurjchem-170	121	9	lc‐nmr	lc‐nmr	PROPN
eurjchem-170	121	10	spectra	spectra	NOUN
eurjchem-170	121	11	.	.	PUNCT
eurjchem-170	122	1	shah	shah	PROPN
eurjchem-170	122	2	et	et	PROPN
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eurjchem-170	122	4	.	.	PUNCT
eurjchem-170	122	5	/	/	SYM
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eurjchem-170	122	8	of	of	ADP
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eurjchem-170	122	10	2	2	NUM
eurjchem-170	122	11	(	(	PUNCT
eurjchem-170	122	12	2	2	NUM
eurjchem-170	122	13	)	)	PUNCT
eurjchem-170	122	14	(	(	PUNCT
eurjchem-170	122	15	2011	2011	NUM
eurjchem-170	122	16	)	)	PUNCT
eurjchem-170	122	17	152‐157	152‐157	NOUN
eurjchem-170	122	18	155	155	NUM
eurjchem-170	123	1	n	n	CCONJ
eurjchem-170	123	2	n	n	NOUN
eurjchem-170	123	3	so	so	ADV
eurjchem-170	123	4	h2o	h2o	NOUN
eurjchem-170	123	5	o	o	NOUN
eurjchem-170	124	1	oh	oh	INTJ
eurjchem-170	124	2	n	n	CCONJ
eurjchem-170	124	3	n	n	NOUN
eurjchem-170	124	4	so	so	ADV
eurjchem-170	124	5	ho	ho	ADJ
eurjchem-170	125	1	o	o	PROPN
eurjchem-170	125	2	oh2	oh2	NOUN
eurjchem-170	125	3	n	n	CCONJ
eurjchem-170	125	4	n	n	PROPN
eurjchem-170	125	5	hso	hso	NOUN
eurjchem-170	125	6	ho	ho	PROPN
eurjchem-170	126	1	o	o	INTJ
eurjchem-170	126	2	oh	oh	INTJ
eurjchem-170	126	3	m	m	PROPN
eurjchem-170	126	4	/	/	SYM
eurjchem-170	126	5	z	z	PROPN
eurjchem-170	126	6	425.1530	425.1530	NUM
eurjchem-170	126	7	n	n	CCONJ
eurjchem-170	126	8	n	n	NOUN
eurjchem-170	126	9	s	s	PART
eurjchem-170	126	10	o	o	NOUN
eurjchem-170	127	1	oh	oh	INTJ
eurjchem-170	127	2	m	m	NOUN
eurjchem-170	127	3	/	/	SYM
eurjchem-170	127	4	z	z	PROPN
eurjchem-170	127	5	379.1475	379.1475	NUM
eurjchem-170	127	6	n	n	CCONJ
eurjchem-170	127	7	n	n	NOUN
eurjchem-170	128	1	so	so	ADV
eurjchem-170	128	2	o	o	INTJ
eurjchem-170	129	1	oh	oh	INTJ
eurjchem-170	129	2	m	m	PROPN
eurjchem-170	129	3	/	/	SYM
eurjchem-170	129	4	z	z	PROPN
eurjchem-170	129	5	407.1424	407.1424	NUM
eurjchem-170	129	6	n	n	CCONJ
eurjchem-170	129	7	n	n	NOUN
eurjchem-170	130	1	so	so	ADV
eurjchem-170	130	2	ho	ho	ADJ
eurjchem-170	131	1	o	o	PROPN
eurjchem-170	132	1	m	m	PROPN
eurjchem-170	133	1	/	/	SYM
eurjchem-170	134	1	z	z	PROPN
eurjchem-170	134	2	407.1424	407.1424	NUM
eurjchem-170	134	3	n	n	CCONJ
eurjchem-170	134	4	n	n	NOUN
eurjchem-170	135	1	so	so	ADV
eurjchem-170	135	2	o	o	PROPN
eurjchem-170	135	3	m	m	PROPN
eurjchem-170	135	4	/	/	SYM
eurjchem-170	135	5	z	z	PROPN
eurjchem-170	135	6	389.1318	389.1318	NUM
eurjchem-170	135	7	n	n	NUM
eurjchem-170	135	8	n	n	NOUN
eurjchem-170	135	9	so	so	ADV
eurjchem-170	136	1	ho	ho	PROPN
eurjchem-170	136	2	m	m	PROPN
eurjchem-170	136	3	/	/	SYM
eurjchem-170	136	4	z	z	PROPN
eurjchem-170	136	5	379.1475	379.1475	NUM
eurjchem-170	136	6	n	n	CCONJ
eurjchem-170	136	7	n	n	NOUN
eurjchem-170	136	8	o	o	NOUN
eurjchem-170	136	9	ho	ho	X
eurjchem-170	136	10	o	o	INTJ
eurjchem-170	137	1	oh	oh	INTJ
eurjchem-170	137	2	m	m	PROPN
eurjchem-170	137	3	/	/	SYM
eurjchem-170	137	4	z	z	PROPN
eurjchem-170	137	5	341.1496	341.1496	NUM
eurjchem-170	137	6	n	n	NUM
eurjchem-170	137	7	h	h	NOUN
eurjchem-170	138	1	n	n	NOUN
eurjchem-170	139	1	so	so	ADV
eurjchem-170	139	2	ho	ho	ADJ
eurjchem-170	139	3	o	o	INTJ
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eurjchem-170	140	2	n	n	ADV
eurjchem-170	140	3	nh	nh	PROPN
eurjchem-170	140	4	so	so	ADV
eurjchem-170	140	5	h2o	h2o	PROPN
eurjchem-170	140	6	m	m	PROPN
eurjchem-170	140	7	/	/	SYM
eurjchem-170	140	8	z	z	PROPN
eurjchem-170	140	9	291.1162	291.1162	NUM
eurjchem-170	140	10	n	n	X
eurjchem-170	140	11	nh	nh	PROPN
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eurjchem-170	140	13	m	m	PROPN
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eurjchem-170	140	15	z	z	PROPN
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eurjchem-170	140	17	n	n	NUM
eurjchem-170	140	18	nh	nh	PROPN
eurjchem-170	140	19	s	s	PART
eurjchem-170	140	20	m	m	PROPN
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eurjchem-170	140	22	z	z	PROPN
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eurjchem-170	140	24	n	n	CCONJ
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eurjchem-170	141	4	z	z	PROPN
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eurjchem-170	141	6	n	n	NOUN
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eurjchem-170	141	8	o	o	NOUN
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eurjchem-170	141	12	z	z	PROPN
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eurjchem-170	141	19	z	z	NOUN
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eurjchem-170	141	21	n	n	PROPN
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eurjchem-170	141	23	m	m	PROPN
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eurjchem-170	141	25	z	z	PROPN
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eurjchem-170	142	8	n	n	PRON
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eurjchem-170	143	5	z	z	PROPN
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eurjchem-170	143	7	n	n	PROPN
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eurjchem-170	144	4	z	z	PROPN
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eurjchem-170	145	8	/	/	SYM
eurjchem-170	145	9	z	z	PROPN
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eurjchem-170	155	1	[	[	X
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eurjchem-170	160	1	[	[	X
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eurjchem-170	161	1	[	[	X
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eurjchem-170	163	1	[	[	X
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eurjchem-170	165	1	[	[	X
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eurjchem-170	165	3	]	]	X
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eurjchem-170	167	1	[	[	X
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eurjchem-170	169	21	h‐13	h‐13	NOUN
eurjchem-170	169	22	had	have	AUX
eurjchem-170	169	23	changed	change	VERB
eurjchem-170	169	24	significantly	significantly	ADV
eurjchem-170	169	25	.	.	PUNCT
eurjchem-170	170	1	this	this	PRON
eurjchem-170	170	2	was	be	AUX
eurjchem-170	170	3	only	only	ADV
eurjchem-170	170	4	possible	possible	ADJ
eurjchem-170	170	5	if	if	SCONJ
eurjchem-170	170	6	the	the	DET
eurjchem-170	170	7	drug	drug	NOUN
eurjchem-170	170	8	(	(	PUNCT
eurjchem-170	170	9	e	e	NOUN
eurjchem-170	170	10	form	form	NOUN
eurjchem-170	170	11	)	)	PUNCT
eurjchem-170	170	12	was	be	AUX
eurjchem-170	170	13	converted	convert	VERB
eurjchem-170	170	14	to	to	ADP
eurjchem-170	170	15	z	z	PROPN
eurjchem-170	170	16	isomer	isomer	PROPN
eurjchem-170	170	17	.	.	PUNCT
eurjchem-170	171	1	due	due	ADP
eurjchem-170	171	2	to	to	ADP
eurjchem-170	171	3	this	this	DET
eurjchem-170	171	4	geometric	geometric	ADJ
eurjchem-170	171	5	isomerization	isomerization	NOUN
eurjchem-170	171	6	,	,	PUNCT
eurjchem-170	171	7	d‐orbital	d‐orbital	PUNCT
eurjchem-170	171	8	electrons	electron	NOUN
eurjchem-170	171	9	of	of	ADP
eurjchem-170	171	10	sulfur	sulfur	NOUN
eurjchem-170	171	11	showed	show	VERB
eurjchem-170	171	12	shielding	shielding	NOUN
eurjchem-170	171	13	effect	effect	NOUN
eurjchem-170	171	14	to	to	ADP
eurjchem-170	171	15	vinyl	vinyl	NOUN
eurjchem-170	171	16	h‐13	h‐13	NOUN
eurjchem-170	171	17	.	.	PUNCT
eurjchem-170	172	1	moreover	moreover	ADV
eurjchem-170	172	2	,	,	PUNCT
eurjchem-170	172	3	observed	observe	VERB
eurjchem-170	172	4	minor	minor	ADJ
eurjchem-170	172	5	change	change	NOUN
eurjchem-170	172	6	in	in	ADP
eurjchem-170	172	7	j	j	PROPN
eurjchem-170	172	8	value	value	NOUN
eurjchem-170	172	9	of	of	ADP
eurjchem-170	172	10	h‐18	h‐18	NOUN
eurjchem-170	172	11	might	might	AUX
eurjchem-170	172	12	be	be	AUX
eurjchem-170	172	13	due	due	ADJ
eurjchem-170	172	14	this	this	DET
eurjchem-170	172	15	spatial	spatial	ADJ
eurjchem-170	172	16	non‐bonding	non‐bonde	VERB
eurjchem-170	172	17	interaction	interaction	NOUN
eurjchem-170	172	18	.	.	PUNCT
eurjchem-170	173	1	the	the	DET
eurjchem-170	173	2	supposition	supposition	NOUN
eurjchem-170	173	3	of	of	ADP
eurjchem-170	173	4	isomerization	isomerization	NOUN
eurjchem-170	173	5	was	be	AUX
eurjchem-170	173	6	verified	verify	VERB
eurjchem-170	173	7	through	through	ADP
eurjchem-170	173	8	correlation	correlation	NOUN
eurjchem-170	173	9	of	of	ADP
eurjchem-170	173	10	the	the	DET
eurjchem-170	173	11	observed	observe	VERB
eurjchem-170	173	12	differential	differential	NOUN
eurjchem-170	173	13	ms	ms	PROPN
eurjchem-170	173	14	peak	peak	NOUN
eurjchem-170	173	15	intensities	intensity	NOUN
eurjchem-170	173	16	of	of	ADP
eurjchem-170	173	17	the	the	DET
eurjchem-170	173	18	drug	drug	NOUN
eurjchem-170	173	19	and	and	CCONJ
eurjchem-170	173	20	the	the	DET
eurjchem-170	173	21	product	product	NOUN
eurjchem-170	173	22	(	(	PUNCT
eurjchem-170	173	23	figure	figure	NOUN
eurjchem-170	173	24	2a	2a	NUM
eurjchem-170	173	25	and	and	CCONJ
eurjchem-170	173	26	2b	2b	NOUN
eurjchem-170	173	27	)	)	PUNCT
eurjchem-170	173	28	,	,	PUNCT
eurjchem-170	173	29	considering	consider	VERB
eurjchem-170	173	30	that	that	SCONJ
eurjchem-170	173	31	isomers	isomer	NOUN
eurjchem-170	173	32	are	be	AUX
eurjchem-170	173	33	known	know	VERB
eurjchem-170	173	34	to	to	PART
eurjchem-170	173	35	show	show	VERB
eurjchem-170	173	36	different	different	ADJ
eurjchem-170	173	37	fragment	fragment	NOUN
eurjchem-170	173	38	ion	ion	NOUN
eurjchem-170	173	39	intensities	intensity	NOUN
eurjchem-170	173	40	[	[	X
eurjchem-170	173	41	16,17	16,17	NUM
eurjchem-170	173	42	]	]	PUNCT
eurjchem-170	173	43	.	.	PUNCT
eurjchem-170	174	1	as	as	SCONJ
eurjchem-170	174	2	discussed	discuss	VERB
eurjchem-170	174	3	under	under	ADP
eurjchem-170	174	4	section	section	NOUN
eurjchem-170	174	5	3.4	3.4	NUM
eurjchem-170	174	6	,	,	PUNCT
eurjchem-170	174	7	the	the	DET
eurjchem-170	174	8	intensity	intensity	NOUN
eurjchem-170	174	9	of	of	ADP
eurjchem-170	174	10	mass	mass	ADJ
eurjchem-170	174	11	peaks	peak	NOUN
eurjchem-170	174	12	of	of	ADP
eurjchem-170	174	13	m	m	PROPN
eurjchem-170	174	14	/	/	SYM
eurjchem-170	174	15	z	z	PROPN
eurjchem-170	174	16	207	207	NUM
eurjchem-170	174	17	and	and	CCONJ
eurjchem-170	174	18	m	m	PROPN
eurjchem-170	174	19	/	/	SYM
eurjchem-170	174	20	z	z	PROPN
eurjchem-170	174	21	341	341	NUM
eurjchem-170	174	22	were	be	AUX
eurjchem-170	174	23	significantly	significantly	ADV
eurjchem-170	174	24	less	less	ADJ
eurjchem-170	174	25	in	in	ADP
eurjchem-170	174	26	case	case	NOUN
eurjchem-170	174	27	of	of	ADP
eurjchem-170	174	28	the	the	DET
eurjchem-170	174	29	product	product	NOUN
eurjchem-170	174	30	.	.	PUNCT
eurjchem-170	175	1	this	this	PRON
eurjchem-170	175	2	was	be	AUX
eurjchem-170	175	3	perhaps	perhaps	ADV
eurjchem-170	175	4	due	due	ADJ
eurjchem-170	175	5	to	to	ADP
eurjchem-170	175	6	hindered	hinder	VERB
eurjchem-170	175	7	protonation	protonation	NOUN
eurjchem-170	175	8	of	of	ADP
eurjchem-170	175	9	thiophene	thiophene	NOUN
eurjchem-170	175	10	ring	ring	NOUN
eurjchem-170	175	11	system	system	NOUN
eurjchem-170	175	12	by	by	ADP
eurjchem-170	175	13	spatial	spatial	ADJ
eurjchem-170	175	14	non‐bonding	non‐bonde	VERB
eurjchem-170	175	15	interaction	interaction	NOUN
eurjchem-170	175	16	of	of	ADP
eurjchem-170	175	17	sulphur	sulphur	NOUN
eurjchem-170	175	18	and	and	CCONJ
eurjchem-170	175	19	vinyl	vinyl	NOUN
eurjchem-170	175	20	hydrogens	hydrogen	NOUN
eurjchem-170	175	21	.	.	PUNCT
eurjchem-170	176	1	in	in	ADP
eurjchem-170	176	2	this	this	DET
eurjchem-170	176	3	circumstance	circumstance	NOUN
eurjchem-170	176	4	,	,	PUNCT
eurjchem-170	176	5	fragmentation	fragmentation	NOUN
eurjchem-170	176	6	from	from	ADP
eurjchem-170	176	7	other	other	ADJ
eurjchem-170	176	8	site	site	NOUN
eurjchem-170	176	9	(	(	PUNCT
eurjchem-170	176	10	route	route	NOUN
eurjchem-170	176	11	four	four	NUM
eurjchem-170	176	12	;	;	PUNCT
eurjchem-170	176	13	n3‐c6	n3‐c6	NOUN
eurjchem-170	176	14	;	;	PUNCT
eurjchem-170	176	15	figure	figure	NOUN
eurjchem-170	176	16	3	3	NUM
eurjchem-170	176	17	)	)	PUNCT
eurjchem-170	176	18	could	could	AUX
eurjchem-170	176	19	be	be	AUX
eurjchem-170	176	20	preferred	prefer	VERB
eurjchem-170	176	21	,	,	PUNCT
eurjchem-170	176	22	and	and	CCONJ
eurjchem-170	176	23	this	this	DET
eurjchem-170	176	24	phenomenon	phenomenon	NOUN
eurjchem-170	176	25	was	be	AUX
eurjchem-170	176	26	clearly	clearly	ADV
eurjchem-170	176	27	seen	see	VERB
eurjchem-170	176	28	from	from	ADP
eurjchem-170	176	29	the	the	DET
eurjchem-170	176	30	observed	observe	VERB
eurjchem-170	176	31	higher	high	ADJ
eurjchem-170	176	32	intensity	intensity	NOUN
eurjchem-170	176	33	of	of	ADP
eurjchem-170	176	34	the	the	DET
eurjchem-170	176	35	ion	ion	NOUN
eurjchem-170	176	36	of	of	ADP
eurjchem-170	176	37	m	m	PROPN
eurjchem-170	176	38	/	/	SYM
eurjchem-170	176	39	z	z	PROPN
eurjchem-170	176	40	273	273	NUM
eurjchem-170	176	41	for	for	ADP
eurjchem-170	176	42	the	the	DET
eurjchem-170	176	43	product	product	NOUN
eurjchem-170	176	44	.	.	PUNCT
eurjchem-170	177	1	incidentally	incidentally	ADV
eurjchem-170	177	2	,	,	PUNCT
eurjchem-170	177	3	a	a	DET
eurjchem-170	177	4	similar	similar	ADJ
eurjchem-170	177	5	observation	observation	NOUN
eurjchem-170	177	6	was	be	AUX
eurjchem-170	177	7	made	make	VERB
eurjchem-170	177	8	by	by	ADP
eurjchem-170	177	9	brum	brum	PROPN
eurjchem-170	177	10	et	et	PROPN
eurjchem-170	177	11	al	al	PROPN
eurjchem-170	177	12	.	.	PROPN
eurjchem-170	178	1	in	in	ADP
eurjchem-170	178	2	ms	ms	PROPN
eurjchem-170	178	3	study	study	NOUN
eurjchem-170	178	4	on	on	ADP
eurjchem-170	178	5	e	e	PROPN
eurjchem-170	178	6	and	and	CCONJ
eurjchem-170	178	7	z	z	NOUN
eurjchem-170	178	8	isomers	isomer	NOUN
eurjchem-170	178	9	of	of	ADP
eurjchem-170	178	10	eprosartan	eprosartan	PROPN
eurjchem-170	178	11	carried	carry	VERB
eurjchem-170	178	12	out	out	ADP
eurjchem-170	178	13	in	in	ADP
eurjchem-170	178	14	apci	apci	ADJ
eurjchem-170	178	15	mode	mode	NOUN
eurjchem-170	178	16	through	through	ADP
eurjchem-170	178	17	direct	direct	ADJ
eurjchem-170	178	18	injection	injection	NOUN
eurjchem-170	178	19	[	[	X
eurjchem-170	178	20	18	18	NUM
eurjchem-170	178	21	]	]	PUNCT
eurjchem-170	178	22	.	.	PUNCT
eurjchem-170	179	1	this	this	PRON
eurjchem-170	179	2	further	far	ADV
eurjchem-170	179	3	strengthens	strengthen	VERB
eurjchem-170	179	4	the	the	DET
eurjchem-170	179	5	identity	identity	NOUN
eurjchem-170	179	6	of	of	ADP
eurjchem-170	179	7	degradation	degradation	NOUN
eurjchem-170	179	8	product	product	NOUN
eurjchem-170	179	9	formed	form	VERB
eurjchem-170	179	10	in	in	ADP
eurjchem-170	179	11	photo	photo	NOUN
eurjchem-170	179	12	alkali	alkali	ADJ
eurjchem-170	179	13	condition	condition	NOUN
eurjchem-170	179	14	as	as	SCONJ
eurjchem-170	179	15	discussed	discuss	VERB
eurjchem-170	179	16	above	above	ADV
eurjchem-170	179	17	.	.	PUNCT
eurjchem-170	180	1	the	the	DET
eurjchem-170	180	2	elucidated	elucidated	ADJ
eurjchem-170	180	3	structure	structure	NOUN
eurjchem-170	180	4	is	be	AUX
eurjchem-170	180	5	further	far	ADV
eurjchem-170	180	6	supported	support	VERB
eurjchem-170	180	7	by	by	ADP
eurjchem-170	180	8	the	the	DET
eurjchem-170	180	9	mechanism	mechanism	NOUN
eurjchem-170	180	10	of	of	ADP
eurjchem-170	180	11	isomerization	isomerization	NOUN
eurjchem-170	180	12	,	,	PUNCT
eurjchem-170	180	13	outlined	outline	VERB
eurjchem-170	180	14	in	in	ADP
eurjchem-170	180	15	figure	figure	NOUN
eurjchem-170	180	16	5	5	NUM
eurjchem-170	180	17	.	.	PUNCT
eurjchem-170	181	1	it	it	PRON
eurjchem-170	181	2	is	be	AUX
eurjchem-170	181	3	postulated	postulate	VERB
eurjchem-170	181	4	that	that	SCONJ
eurjchem-170	181	5	eprosartan	eprosartan	PROPN
eurjchem-170	181	6	(	(	PUNCT
eurjchem-170	181	7	e‐isomer	e‐isomer	NUM
eurjchem-170	181	8	)	)	PUNCT
eurjchem-170	181	9	is	be	AUX
eurjchem-170	181	10	converted	convert	VERB
eurjchem-170	181	11	to	to	ADP
eurjchem-170	181	12	z‐isomer	z‐isomer	X
eurjchem-170	181	13	under	under	ADP
eurjchem-170	181	14	photo	photo	NOUN
eurjchem-170	181	15	alkali	alkali	ADJ
eurjchem-170	181	16	condition	condition	NOUN
eurjchem-170	181	17	through	through	ADP
eurjchem-170	181	18	ionization	ionization	NOUN
eurjchem-170	181	19	of	of	ADP
eurjchem-170	181	20	carboxyl	carboxyl	NOUN
eurjchem-170	181	21	group	group	NOUN
eurjchem-170	181	22	,	,	PUNCT
eurjchem-170	181	23	which	which	PRON
eurjchem-170	181	24	stabilizes	stabilize	VERB
eurjchem-170	181	25	the	the	DET
eurjchem-170	181	26	radical	radical	NOUN
eurjchem-170	181	27	formed	form	VERB
eurjchem-170	181	28	during	during	ADP
eurjchem-170	181	29	the	the	DET
eurjchem-170	181	30	transition	transition	NOUN
eurjchem-170	181	31	state	state	NOUN
eurjchem-170	181	32	.	.	PUNCT
eurjchem-170	182	1	the	the	DET
eurjchem-170	182	2	geometrical	geometrical	ADJ
eurjchem-170	182	3	conversion	conversion	NOUN
eurjchem-170	182	4	(	(	PUNCT
eurjchem-170	182	5	cis	cis	NOUN
eurjchem-170	182	6	to	to	ADP
eurjchem-170	182	7	trans	tran	NOUN
eurjchem-170	182	8	)	)	PUNCT
eurjchem-170	182	9	of	of	ADP
eurjchem-170	182	10	vinyl	vinyl	NOUN
eurjchem-170	182	11	compounds	compound	NOUN
eurjchem-170	182	12	on	on	ADP
eurjchem-170	182	13	exposure	exposure	NOUN
eurjchem-170	182	14	to	to	ADP
eurjchem-170	182	15	light	light	NOUN
eurjchem-170	182	16	is	be	AUX
eurjchem-170	182	17	known	know	VERB
eurjchem-170	182	18	previously	previously	ADV
eurjchem-170	182	19	[	[	X
eurjchem-170	182	20	19,20	19,20	NOUN
eurjchem-170	182	21	]	]	X
eurjchem-170	182	22	.	.	PUNCT
eurjchem-170	183	1	4	4	X
eurjchem-170	183	2	.	.	X
eurjchem-170	183	3	conclusion	conclusion	NOUN
eurjchem-170	183	4	this	this	DET
eurjchem-170	183	5	systematic	systematic	ADJ
eurjchem-170	183	6	stress	stress	NOUN
eurjchem-170	183	7	degradation	degradation	NOUN
eurjchem-170	183	8	study	study	NOUN
eurjchem-170	183	9	on	on	ADP
eurjchem-170	183	10	eprosartan	eprosartan	PROPN
eurjchem-170	183	11	,	,	PUNCT
eurjchem-170	183	12	carried	carry	VERB
eurjchem-170	183	13	out	out	ADP
eurjchem-170	183	14	according	accord	VERB
eurjchem-170	183	15	to	to	ADP
eurjchem-170	183	16	ich	ich	PROPN
eurjchem-170	183	17	/	/	SYM
eurjchem-170	183	18	who	who	PRON
eurjchem-170	183	19	guidelines	guideline	VERB
eurjchem-170	183	20	,	,	PUNCT
eurjchem-170	183	21	reveals	reveal	VERB
eurjchem-170	183	22	that	that	SCONJ
eurjchem-170	183	23	the	the	DET
eurjchem-170	183	24	drug	drug	NOUN
eurjchem-170	183	25	is	be	AUX
eurjchem-170	183	26	stable	stable	ADJ
eurjchem-170	183	27	to	to	ADP
eurjchem-170	183	28	hydrolysis	hydrolysis	NOUN
eurjchem-170	183	29	,	,	PUNCT
eurjchem-170	183	30	oxidation	oxidation	NOUN
eurjchem-170	183	31	,	,	PUNCT
eurjchem-170	183	32	thermal	thermal	ADJ
eurjchem-170	183	33	stress	stress	NOUN
eurjchem-170	183	34	and	and	CCONJ
eurjchem-170	183	35	even	even	ADV
eurjchem-170	183	36	to	to	PART
eurjchem-170	183	37	light	light	NOUN
eurjchem-170	183	38	in	in	ADP
eurjchem-170	183	39	solid	solid	ADJ
eurjchem-170	183	40	state	state	NOUN
eurjchem-170	183	41	and	and	CCONJ
eurjchem-170	183	42	in	in	ADP
eurjchem-170	183	43	neutral	neutral	ADJ
eurjchem-170	183	44	and	and	CCONJ
eurjchem-170	183	45	acid	acid	ADJ
eurjchem-170	183	46	solutions	solution	NOUN
eurjchem-170	183	47	.	.	PUNCT
eurjchem-170	184	1	it	it	PRON
eurjchem-170	184	2	is	be	AUX
eurjchem-170	184	3	only	only	ADV
eurjchem-170	184	4	unstable	unstable	ADJ
eurjchem-170	184	5	in	in	ADP
eurjchem-170	184	6	photo	photo	NOUN
eurjchem-170	184	7	alkaline	alkaline	NOUN
eurjchem-170	184	8	solutions	solution	NOUN
eurjchem-170	184	9	.	.	PUNCT
eurjchem-170	185	1	the	the	DET
eurjchem-170	185	2	degradation	degradation	NOUN
eurjchem-170	185	3	product	product	NOUN
eurjchem-170	185	4	is	be	AUX
eurjchem-170	185	5	characterized	characterize	VERB
eurjchem-170	185	6	through	through	ADP
eurjchem-170	185	7	complementary	complementary	ADJ
eurjchem-170	185	8	use	use	NOUN
eurjchem-170	185	9	of	of	ADP
eurjchem-170	185	10	hyphenated	hyphenated	ADJ
eurjchem-170	185	11	lc‐	lc‐	ADJ
eurjchem-170	185	12	ms	ms	NOUN
eurjchem-170	185	13	and	and	CCONJ
eurjchem-170	185	14	lc‐nmr	lc‐nmr	PROPN
eurjchem-170	185	15	techniques	technique	NOUN
eurjchem-170	185	16	as	as	ADP
eurjchem-170	185	17	z‐isomer	z‐isomer	NUM
eurjchem-170	185	18	of	of	ADP
eurjchem-170	185	19	the	the	DET
eurjchem-170	185	20	drug	drug	NOUN
eurjchem-170	185	21	(	(	PUNCT
eurjchem-170	185	22	(	(	PUNCT
eurjchem-170	185	23	z)‐4‐((2‐	z)‐4‐((2‐	X
eurjchem-170	185	24	butyl‐5‐(2‐carboxy‐3‐(thiophen‐2‐yl)prop‐1‐enyl)‐1h‐	butyl‐5‐(2‐carboxy‐3‐(thiophen‐2‐yl)prop‐1‐enyl)‐1h‐	ADJ
eurjchem-170	185	25	156	156	NUM
eurjchem-170	185	26	shah	shah	NOUN
eurjchem-170	185	27	et	et	PROPN
eurjchem-170	185	28	al	al	PROPN
eurjchem-170	185	29	.	.	PUNCT
eurjchem-170	185	30	/	/	SYM
eurjchem-170	185	31	european	european	PROPN
eurjchem-170	185	32	journal	journal	PROPN
eurjchem-170	185	33	of	of	ADP
eurjchem-170	185	34	chemistry	chemistry	NOUN
eurjchem-170	185	35	2	2	NUM
eurjchem-170	185	36	(	(	PUNCT
eurjchem-170	185	37	2	2	NUM
eurjchem-170	185	38	)	)	PUNCT
eurjchem-170	185	39	(	(	PUNCT
eurjchem-170	185	40	2011	2011	NUM
eurjchem-170	185	41	)	)	PUNCT
eurjchem-170	185	42	152‐157	152‐157	NUM
eurjchem-170	185	43	table	table	NOUN
eurjchem-170	185	44	1	1	NUM
eurjchem-170	185	45	.	.	PUNCT
eurjchem-170	186	1	ms	ms	PROPN
eurjchem-170	186	2	/	/	SYM
eurjchem-170	186	3	tof	tof	PROPN
eurjchem-170	186	4	data	datum	NOUN
eurjchem-170	186	5	and	and	CCONJ
eurjchem-170	186	6	relative	relative	ADJ
eurjchem-170	186	7	ion	ion	NOUN
eurjchem-170	186	8	intensities	intensity	NOUN
eurjchem-170	186	9	of	of	ADP
eurjchem-170	186	10	the	the	DET
eurjchem-170	186	11	drug	drug	NOUN
eurjchem-170	186	12	and	and	CCONJ
eurjchem-170	186	13	the	the	DET
eurjchem-170	186	14	product	product	NOUN
eurjchem-170	186	15	along	along	ADP
eurjchem-170	186	16	with	with	ADP
eurjchem-170	186	17	msn	msn	PROPN
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eurjchem-170	189	2	m+h]+	m+h]+	NOUN
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eurjchem-170	190	7	‐	‐	ADV
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eurjchem-170	190	24	)	)	PUNCT
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eurjchem-170	190	26	[	[	X
eurjchem-170	190	27	m+h]+	m+h]+	PROPN
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eurjchem-170	190	29	h2o	h2o	PROPN
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eurjchem-170	191	28	a	a	DET
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eurjchem-170	192	2	m+h]+	m+h]+	PROPN
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eurjchem-170	192	44	)	)	PUNCT
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eurjchem-170	194	43	)	)	PUNCT
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eurjchem-170	196	27	)	)	PUNCT
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eurjchem-170	197	16	‐2.1	‐2.1	NOUN
eurjchem-170	197	17	)	)	PUNCT
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eurjchem-170	197	19	m	m	NOUN
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eurjchem-170	197	24	1	1	NUM
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eurjchem-170	197	29	(	(	PUNCT
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eurjchem-170	197	31	;	;	PUNCT
eurjchem-170	197	32	4.8	4.8	NUM
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eurjchem-170	197	34	c8h7o2	c8h7o2	PROPN
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eurjchem-170	197	38	‐0.4	‐0.4	NUM
eurjchem-170	197	39	)	)	PUNCT
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eurjchem-170	198	1	[	[	X
eurjchem-170	198	2	m+h]+	m+h]+	NOUN
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eurjchem-170	198	4	c15h18n2o2s	c15h18n2o2s	NOUN
eurjchem-170	198	5	c15h18n2o4	c15h18n2o4	NOUN
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eurjchem-170	198	7	1	1	NUM
eurjchem-170	198	8	a‐h	a‐h	NOUN
eurjchem-170	198	9	:	:	PUNCT
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eurjchem-170	198	15	2a	2a	NUM
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eurjchem-170	200	44	,	,	PUNCT
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eurjchem-170	200	49	297	297	NUM
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eurjchem-170	201	9	product	product	NOUN
eurjchem-170	201	10	along	along	ADP
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eurjchem-170	201	13	,	,	PUNCT
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eurjchem-170	201	15	constants	constant	NOUN
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eurjchem-170	202	4	δh	δh	X
eurjchem-170	202	5	/	/	SYM
eurjchem-170	202	6	ppm	ppm	ADJ
eurjchem-170	202	7	(	(	PUNCT
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eurjchem-170	202	9	,	,	PUNCT
eurjchem-170	202	10	j	j	PROPN
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eurjchem-170	202	13	hz	hz	ADJ
eurjchem-170	202	14	)	)	PUNCT
eurjchem-170	202	15	cosy	cosy	ADJ
eurjchem-170	202	16	δh	δh	X
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eurjchem-170	202	18	ppm	ppm	ADJ
eurjchem-170	202	19	(	(	PUNCT
eurjchem-170	202	20	multiplicity	multiplicity	NOUN
eurjchem-170	202	21	,	,	PUNCT
eurjchem-170	202	22	j	j	PROPN
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eurjchem-170	202	24	in	in	ADP
eurjchem-170	202	25	hz	hz	ADJ
eurjchem-170	202	26	)	)	PUNCT
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eurjchem-170	202	28	5	5	NUM
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eurjchem-170	202	30	(	(	PUNCT
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eurjchem-170	202	32	)	)	PUNCT
eurjchem-170	202	33	‐	‐	ADV
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eurjchem-170	202	35	(	(	PUNCT
eurjchem-170	202	36	s	s	NOUN
eurjchem-170	202	37	)	)	PUNCT
eurjchem-170	202	38	‐	‐	ADV
eurjchem-170	202	39	6	6	NUM
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eurjchem-170	202	41	(	(	PUNCT
eurjchem-170	202	42	s	s	NOUN
eurjchem-170	202	43	)	)	PUNCT
eurjchem-170	202	44	‐	‐	ADV
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eurjchem-170	202	46	(	(	PUNCT
eurjchem-170	202	47	s	s	NOUN
eurjchem-170	202	48	)	)	PUNCT
eurjchem-170	202	49	‐	‐	ADV
eurjchem-170	202	50	8	8	NUM
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eurjchem-170	202	52	(	(	PUNCT
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eurjchem-170	202	54	,	,	PUNCT
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eurjchem-170	202	57	h‐9	h‐9	ADP
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eurjchem-170	202	75	d	d	NOUN
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eurjchem-170	202	78	)	)	PUNCT
eurjchem-170	202	79	h‐8	h‐8	NOUN
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eurjchem-170	202	84	,	,	PUNCT
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eurjchem-170	202	86	)	)	PUNCT
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eurjchem-170	202	94	h‐12	h‐12	VERB
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eurjchem-170	202	99	,	,	PUNCT
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eurjchem-170	202	101	)	)	PUNCT
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eurjchem-170	202	138	)	)	PUNCT
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eurjchem-170	202	158	)	)	PUNCT
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eurjchem-170	202	168	)	)	PUNCT
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eurjchem-170	203	4	d	d	PROPN
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eurjchem-170	203	7	)	)	PUNCT
eurjchem-170	203	8	h‐19	h‐19	VERB
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eurjchem-170	203	35	,	,	PUNCT
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eurjchem-170	203	50	(	(	PUNCT
eurjchem-170	203	51	m	m	NOUN
eurjchem-170	203	52	)	)	PUNCT
eurjchem-170	203	53	h‐2	h‐2	NOUN
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eurjchem-170	203	55	,	,	PUNCT
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eurjchem-170	203	76	’	'	PUNCT
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eurjchem-170	203	80	,	,	PUNCT
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eurjchem-170	203	82	)	)	PUNCT
eurjchem-170	203	83	h‐3	h‐3	NOUN
eurjchem-170	203	84	’	'	PUNCT
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eurjchem-170	203	94	2	2	NUM
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eurjchem-170	203	100	)	)	PUNCT
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eurjchem-170	204	5	.	.	NOUN
eurjchem-170	204	6	1h	1h	NUM
eurjchem-170	204	7	lc‐nmr	lc‐nmr	PROPN
eurjchem-170	204	8	spectra	spectra	NOUN
eurjchem-170	204	9	of	of	ADP
eurjchem-170	204	10	the	the	DET
eurjchem-170	204	11	drug	drug	NOUN
eurjchem-170	204	12	(	(	PUNCT
eurjchem-170	204	13	upper	upper	ADJ
eurjchem-170	204	14	)	)	PUNCT
eurjchem-170	204	15	and	and	CCONJ
eurjchem-170	204	16	the	the	DET
eurjchem-170	204	17	product	product	NOUN
eurjchem-170	204	18	(	(	PUNCT
eurjchem-170	204	19	lower	low	ADJ
eurjchem-170	204	20	)	)	PUNCT
eurjchem-170	204	21	.	.	PUNCT
eurjchem-170	205	1	figure	figure	NOUN
eurjchem-170	205	2	5	5	NUM
eurjchem-170	205	3	.	.	PUNCT
eurjchem-170	206	1	mechanism	mechanism	NOUN
eurjchem-170	206	2	of	of	ADP
eurjchem-170	206	3	formation	formation	NOUN
eurjchem-170	206	4	of	of	ADP
eurjchem-170	206	5	z‐isomer	z‐isomer	NUM
eurjchem-170	206	6	from	from	ADP
eurjchem-170	206	7	the	the	DET
eurjchem-170	206	8	drug	drug	NOUN
eurjchem-170	206	9	.	.	PUNCT
eurjchem-170	207	1	imidazol‐1‐yl)ethyl)benzoic	imidazol‐1‐yl)ethyl)benzoic	VERB
eurjchem-170	207	2	acid	acid	NOUN
eurjchem-170	207	3	)	)	PUNCT
eurjchem-170	207	4	.	.	PUNCT
eurjchem-170	208	1	though	though	SCONJ
eurjchem-170	208	2	it	it	PRON
eurjchem-170	208	3	is	be	AUX
eurjchem-170	208	4	a	a	DET
eurjchem-170	208	5	reported	report	VERB
eurjchem-170	208	6	photolytic	photolytic	ADJ
eurjchem-170	208	7	product	product	NOUN
eurjchem-170	208	8	of	of	ADP
eurjchem-170	208	9	eprosartan	eprosartan	PROPN
eurjchem-170	208	10	,	,	PUNCT
eurjchem-170	208	11	the	the	DET
eurjchem-170	208	12	exact	exact	ADJ
eurjchem-170	208	13	condition	condition	NOUN
eurjchem-170	208	14	under	under	ADP
eurjchem-170	208	15	which	which	PRON
eurjchem-170	208	16	it	it	PRON
eurjchem-170	208	17	is	be	AUX
eurjchem-170	208	18	formed	form	VERB
eurjchem-170	208	19	from	from	ADP
eurjchem-170	208	20	the	the	DET
eurjchem-170	208	21	drug	drug	NOUN
eurjchem-170	208	22	under	under	ADP
eurjchem-170	208	23	light	light	NOUN
eurjchem-170	208	24	is	be	AUX
eurjchem-170	208	25	identified	identify	VERB
eurjchem-170	208	26	here	here	ADV
eurjchem-170	208	27	.	.	PUNCT
eurjchem-170	209	1	the	the	DET
eurjchem-170	209	2	mechanism	mechanism	NOUN
eurjchem-170	209	3	of	of	ADP
eurjchem-170	209	4	formation	formation	NOUN
eurjchem-170	209	5	of	of	ADP
eurjchem-170	209	6	the	the	DET
eurjchem-170	209	7	product	product	NOUN
eurjchem-170	209	8	is	be	AUX
eurjchem-170	209	9	proposed	propose	VERB
eurjchem-170	209	10	.	.	PUNCT
eurjchem-170	210	1	a	a	DET
eurjchem-170	210	2	complete	complete	ADJ
eurjchem-170	210	3	mass	mass	ADJ
eurjchem-170	210	4	fragmentation	fragmentation	NOUN
eurjchem-170	210	5	pathway	pathway	NOUN
eurjchem-170	210	6	of	of	ADP
eurjchem-170	210	7	the	the	DET
eurjchem-170	210	8	drug	drug	NOUN
eurjchem-170	210	9	is	be	AUX
eurjchem-170	210	10	reported	report	VERB
eurjchem-170	210	11	for	for	ADP
eurjchem-170	210	12	the	the	DET
eurjchem-170	210	13	first	first	ADJ
eurjchem-170	210	14	time	time	NOUN
eurjchem-170	210	15	.	.	PUNCT
eurjchem-170	211	1	also	also	ADV
eurjchem-170	211	2	,	,	PUNCT
eurjchem-170	211	3	extensive	extensive	ADJ
eurjchem-170	211	4	ms	ms	NOUN
eurjchem-170	211	5	and	and	CCONJ
eurjchem-170	211	6	nmr	nmr	NOUN
eurjchem-170	211	7	data	datum	NOUN
eurjchem-170	211	8	and	and	CCONJ
eurjchem-170	211	9	their	their	PRON
eurjchem-170	211	10	interpretation	interpretation	NOUN
eurjchem-170	211	11	are	be	AUX
eurjchem-170	211	12	provided	provide	VERB
eurjchem-170	211	13	for	for	ADP
eurjchem-170	211	14	both	both	CCONJ
eurjchem-170	211	15	the	the	DET
eurjchem-170	211	16	drug	drug	NOUN
eurjchem-170	211	17	and	and	CCONJ
eurjchem-170	211	18	the	the	DET
eurjchem-170	211	19	degradation	degradation	NOUN
eurjchem-170	211	20	product	product	NOUN
eurjchem-170	211	21	.	.	PUNCT
eurjchem-170	212	1	the	the	DET
eurjchem-170	212	2	given	give	VERB
eurjchem-170	212	3	information	information	NOUN
eurjchem-170	212	4	can	can	AUX
eurjchem-170	212	5	be	be	AUX
eurjchem-170	212	6	gainfully	gainfully	ADV
eurjchem-170	212	7	exploited	exploit	VERB
eurjchem-170	212	8	in	in	ADP
eurjchem-170	212	9	future	future	ADJ
eurjchem-170	212	10	investigations	investigation	NOUN
eurjchem-170	212	11	on	on	ADP
eurjchem-170	212	12	characterization	characterization	NOUN
eurjchem-170	212	13	of	of	ADP
eurjchem-170	212	14	process	process	NOUN
eurjchem-170	212	15	related	relate	VERB
eurjchem-170	212	16	impurities	impurity	NOUN
eurjchem-170	212	17	,	,	PUNCT
eurjchem-170	212	18	drug‐excipient	drug‐excipient	NOUN
eurjchem-170	212	19	interaction	interaction	NOUN
eurjchem-170	212	20	products	product	NOUN
eurjchem-170	212	21	,	,	PUNCT
eurjchem-170	212	22	and/or	and/or	CCONJ
eurjchem-170	212	23	metabolites	metabolite	NOUN
eurjchem-170	212	24	of	of	ADP
eurjchem-170	212	25	the	the	DET
eurjchem-170	212	26	drug	drug	NOUN
eurjchem-170	212	27	.	.	PUNCT
eurjchem-170	213	1	overall	overall	ADV
eurjchem-170	213	2	,	,	PUNCT
eurjchem-170	213	3	the	the	DET
eurjchem-170	213	4	study	study	NOUN
eurjchem-170	213	5	strengthens	strengthen	VERB
eurjchem-170	213	6	the	the	DET
eurjchem-170	213	7	utility	utility	NOUN
eurjchem-170	213	8	of	of	ADP
eurjchem-170	213	9	hyphenated	hyphenated	ADJ
eurjchem-170	213	10	tools	tool	NOUN
eurjchem-170	213	11	for	for	ADP
eurjchem-170	213	12	characterizing	characterize	VERB
eurjchem-170	213	13	the	the	DET
eurjchem-170	213	14	unknown	unknown	ADJ
eurjchem-170	213	15	products	product	NOUN
eurjchem-170	213	16	formed	form	VERB
eurjchem-170	213	17	in	in	ADP
eurjchem-170	213	18	small	small	ADJ
eurjchem-170	213	19	quantities	quantity	NOUN
eurjchem-170	213	20	during	during	ADP
eurjchem-170	213	21	stability	stability	NOUN
eurjchem-170	213	22	or	or	CCONJ
eurjchem-170	213	23	stress	stress	NOUN
eurjchem-170	213	24	studies	study	NOUN
eurjchem-170	213	25	,	,	PUNCT
eurjchem-170	213	26	against	against	ADP
eurjchem-170	213	27	the	the	DET
eurjchem-170	213	28	use	use	NOUN
eurjchem-170	213	29	of	of	ADP
eurjchem-170	213	30	cumbersome	cumbersome	ADJ
eurjchem-170	213	31	procedure	procedure	NOUN
eurjchem-170	213	32	of	of	ADP
eurjchem-170	213	33	isolation	isolation	NOUN
eurjchem-170	213	34	or	or	CCONJ
eurjchem-170	213	35	synthesis	synthesis	NOUN
eurjchem-170	213	36	.	.	PUNCT
eurjchem-170	214	1	references	reference	NOUN
eurjchem-170	214	2	[	[	X
eurjchem-170	214	3	1	1	NUM
eurjchem-170	214	4	]	]	PUNCT
eurjchem-170	214	5	.	.	PUNCT
eurjchem-170	215	1	ich	ich	NOUN
eurjchem-170	215	2	topic	topic	NOUN
eurjchem-170	215	3	q1a	q1a	NOUN
eurjchem-170	215	4	(	(	PUNCT
eurjchem-170	215	5	r2	r2	PROPN
eurjchem-170	215	6	)	)	PUNCT
eurjchem-170	215	7	,	,	PUNCT
eurjchem-170	215	8	stability	stability	NOUN
eurjchem-170	215	9	testing	testing	NOUN
eurjchem-170	215	10	of	of	ADP
eurjchem-170	215	11	new	new	ADJ
eurjchem-170	215	12	drug	drug	NOUN
eurjchem-170	215	13	substances	substance	NOUN
eurjchem-170	215	14	and	and	CCONJ
eurjchem-170	215	15	products	product	NOUN
eurjchem-170	215	16	,	,	PUNCT
eurjchem-170	215	17	in	in	ADP
eurjchem-170	215	18	:	:	PUNCT
eurjchem-170	215	19	international	international	ADJ
eurjchem-170	215	20	conference	conference	NOUN
eurjchem-170	215	21	on	on	ADP
eurjchem-170	215	22	harmonisation	harmonisation	NOUN
eurjchem-170	215	23	,	,	PUNCT
eurjchem-170	215	24	ifpma	ifpma	NOUN
eurjchem-170	215	25	,	,	PUNCT
eurjchem-170	215	26	geneva	geneva	PROPN
eurjchem-170	215	27	,	,	PUNCT
eurjchem-170	215	28	2003	2003	NUM
eurjchem-170	215	29	.	.	PUNCT
eurjchem-170	216	1	[	[	X
eurjchem-170	216	2	2	2	NUM
eurjchem-170	216	3	]	]	PUNCT
eurjchem-170	216	4	.	.	PUNCT
eurjchem-170	217	1	who	who	PRON
eurjchem-170	217	2	,	,	PUNCT
eurjchem-170	217	3	draft	draft	VERB
eurjchem-170	217	4	stability	stability	NOUN
eurjchem-170	217	5	testing	testing	NOUN
eurjchem-170	217	6	of	of	ADP
eurjchem-170	217	7	active	active	ADJ
eurjchem-170	217	8	pharmaceutical	pharmaceutical	ADJ
eurjchem-170	217	9	ingredients	ingredient	NOUN
eurjchem-170	217	10	and	and	CCONJ
eurjchem-170	217	11	pharmaceutical	pharmaceutical	NOUN
eurjchem-170	217	12	products	product	NOUN
eurjchem-170	217	13	,	,	PUNCT
eurjchem-170	217	14	world	world	NOUN
eurjchem-170	217	15	health	health	NOUN
eurjchem-170	217	16	organization	organization	PROPN
eurjchem-170	217	17	,	,	PUNCT
eurjchem-170	217	18	geneva	geneva	PROPN
eurjchem-170	217	19	,	,	PUNCT
eurjchem-170	217	20	2007	2007	NUM
eurjchem-170	217	21	.	.	PUNCT
eurjchem-170	218	1	[	[	X
eurjchem-170	218	2	3	3	NUM
eurjchem-170	218	3	]	]	PUNCT
eurjchem-170	218	4	.	.	PUNCT
eurjchem-170	219	1	murakami	murakami	NOUN
eurjchem-170	219	2	,	,	PUNCT
eurjchem-170	219	3	t.	t.	PROPN
eurjchem-170	219	4	;	;	PUNCT
eurjchem-170	219	5	kawasaki	kawasaki	PROPN
eurjchem-170	219	6	,	,	PUNCT
eurjchem-170	219	7	t.	t.	PROPN
eurjchem-170	219	8	;	;	PUNCT
eurjchem-170	219	9	takemura	takemura	VERB
eurjchem-170	219	10	,	,	PUNCT
eurjchem-170	219	11	a.	a.	NOUN
eurjchem-170	219	12	;	;	PUNCT
eurjchem-170	219	13	fukutsu	fukutsu	ADJ
eurjchem-170	219	14	,	,	PUNCT
eurjchem-170	219	15	n.	n.	PROPN
eurjchem-170	219	16	;	;	PUNCT
eurjchem-170	219	17	kishi	kishi	PROPN
eurjchem-170	219	18	,	,	PUNCT
eurjchem-170	219	19	n.	n.	PROPN
eurjchem-170	219	20	;	;	PUNCT
eurjchem-170	219	21	kusu	kusu	PROPN
eurjchem-170	219	22	,	,	PUNCT
eurjchem-170	219	23	f.	f.	PROPN
eurjchem-170	219	24	j.	j.	PROPN
eurjchem-170	219	25	chromatogr	chromatogr	PROPN
eurjchem-170	219	26	.	.	PUNCT
eurjchem-170	220	1	a	a	DET
eurjchem-170	220	2	2008	2008	NUM
eurjchem-170	220	3	,	,	PUNCT
eurjchem-170	220	4	1208	1208	NUM
eurjchem-170	220	5	,	,	PUNCT
eurjchem-170	220	6	164‐174	164‐174	NUM
eurjchem-170	220	7	.	.	PUNCT
eurjchem-170	221	1	[	[	X
eurjchem-170	221	2	4	4	NUM
eurjchem-170	221	3	]	]	PUNCT
eurjchem-170	221	4	.	.	PUNCT
eurjchem-170	222	1	shah	shah	PROPN
eurjchem-170	222	2	,	,	PUNCT
eurjchem-170	222	3	r.	r.	PROPN
eurjchem-170	222	4	p.	p.	PROPN
eurjchem-170	222	5	;	;	PUNCT
eurjchem-170	222	6	kumar	kumar	PROPN
eurjchem-170	222	7	,	,	PUNCT
eurjchem-170	222	8	v.	v.	PROPN
eurjchem-170	222	9	;	;	PUNCT
eurjchem-170	222	10	singh	singh	PROPN
eurjchem-170	222	11	,	,	PUNCT
eurjchem-170	222	12	s.	s.	PROPN
eurjchem-170	222	13	rapid	rapid	PROPN
eurjchem-170	222	14	commun	commun	PROPN
eurjchem-170	222	15	.	.	PUNCT
eurjchem-170	223	1	mass	mass	PROPN
eurjchem-170	223	2	spectrom	spectrom	PROPN
eurjchem-170	223	3	.	.	PUNCT
eurjchem-170	224	1	2008	2008	NUM
eurjchem-170	224	2	,	,	PUNCT
eurjchem-170	224	3	22	22	NUM
eurjchem-170	224	4	,	,	PUNCT
eurjchem-170	224	5	613‐622	613‐622	NUM
eurjchem-170	224	6	.	.	PUNCT
eurjchem-170	225	1	[	[	X
eurjchem-170	225	2	5	5	NUM
eurjchem-170	225	3	]	]	PUNCT
eurjchem-170	225	4	.	.	PUNCT
eurjchem-170	226	1	novak	novak	PROPN
eurjchem-170	226	2	,	,	PUNCT
eurjchem-170	226	3	p.	p.	PROPN
eurjchem-170	226	4	;	;	PUNCT
eurjchem-170	226	5	tepes	tepe	NOUN
eurjchem-170	226	6	,	,	PUNCT
eurjchem-170	226	7	p.	p.	NOUN
eurjchem-170	226	8	;	;	PUNCT
eurjchem-170	226	9	ilijas	ilijas	NOUN
eurjchem-170	226	10	,	,	PUNCT
eurjchem-170	226	11	m.	m.	NOUN
eurjchem-170	226	12	;	;	PUNCT
eurjchem-170	226	13	fistric	fistric	NOUN
eurjchem-170	226	14	,	,	PUNCT
eurjchem-170	226	15	i.	i.	NOUN
eurjchem-170	226	16	;	;	PUNCT
eurjchem-170	226	17	bratos	brato	NOUN
eurjchem-170	226	18	,	,	PUNCT
eurjchem-170	226	19	i.	i.	NOUN
eurjchem-170	226	20	;	;	PUNCT
eurjchem-170	226	21	avdagic	avdagic	PROPN
eurjchem-170	226	22	,	,	PUNCT
eurjchem-170	226	23	a.	a.	NOUN
eurjchem-170	226	24	;	;	PUNCT
eurjchem-170	226	25	hamersak	hamersak	PROPN
eurjchem-170	226	26	,	,	PUNCT
eurjchem-170	226	27	z.	z.	PROPN
eurjchem-170	226	28	;	;	PUNCT
eurjchem-170	226	29	markovic	markovic	PROPN
eurjchem-170	226	30	,	,	PUNCT
eurjchem-170	226	31	v.	v.	PROPN
eurjchem-170	226	32	g.	g.	PROPN
eurjchem-170	226	33	;	;	PUNCT
eurjchem-170	226	34	dumic	dumic	ADJ
eurjchem-170	226	35	,	,	PUNCT
eurjchem-170	226	36	m.	m.	NOUN
eurjchem-170	226	37	j.	j.	PROPN
eurjchem-170	226	38	pharm	pharm	PROPN
eurjchem-170	226	39	.	.	PUNCT
eurjchem-170	227	1	biomed	biome	VERB
eurjchem-170	227	2	.	.	PUNCT
eurjchem-170	228	1	anal	anal	ADJ
eurjchem-170	228	2	.	.	PUNCT
eurjchem-170	229	1	2009	2009	NUM
eurjchem-170	229	2	,	,	PUNCT
eurjchem-170	229	3	50	50	NUM
eurjchem-170	229	4	,	,	PUNCT
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eurjchem-170	229	6	.	.	PUNCT
eurjchem-170	230	1	[	[	X
eurjchem-170	230	2	6	6	NUM
eurjchem-170	230	3	]	]	PUNCT
eurjchem-170	230	4	.	.	PUNCT
eurjchem-170	231	1	dev	dev	PROPN
eurjchem-170	231	2	,	,	PUNCT
eurjchem-170	231	3	r.	r.	PROPN
eurjchem-170	231	4	v.	v.	PROPN
eurjchem-170	231	5	;	;	PUNCT
eurjchem-170	231	6	kiran	kiran	PROPN
eurjchem-170	231	7	,	,	PUNCT
eurjchem-170	231	8	g.	g.	PROPN
eurjchem-170	231	9	s.	s.	PROPN
eurjchem-170	231	10	u.	u.	PROPN
eurjchem-170	231	11	;	;	PUNCT
eurjchem-170	231	12	subbaiah	subbaiah	PROPN
eurjchem-170	231	13	,	,	PUNCT
eurjchem-170	231	14	b.	b.	PROPN
eurjchem-170	231	15	v.	v.	PROPN
eurjchem-170	231	16	;	;	PUNCT
eurjchem-170	231	17	babu	babu	PROPN
eurjchem-170	231	18	,	,	PUNCT
eurjchem-170	231	19	b.	b.	PROPN
eurjchem-170	231	20	s.	s.	PROPN
eurjchem-170	231	21	;	;	PUNCT
eurjchem-170	231	22	babu	babu	PROPN
eurjchem-170	231	23	,	,	PUNCT
eurjchem-170	231	24	j.	j.	PROPN
eurjchem-170	231	25	m.	m.	PROPN
eurjchem-170	231	26	;	;	PUNCT
eurjchem-170	231	27	dubey	dubey	PROPN
eurjchem-170	231	28	,	,	PUNCT
eurjchem-170	231	29	p.	p.	PROPN
eurjchem-170	231	30	k.	k.	PROPN
eurjchem-170	231	31	;	;	PUNCT
eurjchem-170	231	32	vyas	vyas	PROPN
eurjchem-170	231	33	,	,	PUNCT
eurjchem-170	231	34	k.	k.	PROPN
eurjchem-170	231	35	magn	magn	PROPN
eurjchem-170	231	36	.	.	PUNCT
eurjchem-170	232	1	reson	reson	PROPN
eurjchem-170	232	2	.	.	PUNCT
eurjchem-170	233	1	chem	chem	PROPN
eurjchem-170	233	2	.	.	PUNCT
eurjchem-170	234	1	2009	2009	NUM
eurjchem-170	234	2	,	,	PUNCT
eurjchem-170	234	3	47	47	NUM
eurjchem-170	234	4	,	,	PUNCT
eurjchem-170	234	5	443‐448	443‐448	NUM
eurjchem-170	234	6	.	.	PUNCT
eurjchem-170	235	1	[	[	X
eurjchem-170	235	2	7	7	NUM
eurjchem-170	235	3	]	]	PUNCT
eurjchem-170	235	4	.	.	PUNCT
eurjchem-170	235	5	shah	shah	PROPN
eurjchem-170	235	6	,	,	PUNCT
eurjchem-170	235	7	r.	r.	PROPN
eurjchem-170	235	8	p.	p.	PROPN
eurjchem-170	235	9	;	;	PUNCT
eurjchem-170	235	10	sahu	sahu	PROPN
eurjchem-170	235	11	,	,	PUNCT
eurjchem-170	235	12	a.	a.	NOUN
eurjchem-170	235	13	;	;	PUNCT
eurjchem-170	235	14	singh	singh	PROPN
eurjchem-170	235	15	,	,	PUNCT
eurjchem-170	235	16	s.	s.	PROPN
eurjchem-170	235	17	j.	j.	PROPN
eurjchem-170	235	18	pharm	pharm	PROPN
eurjchem-170	235	19	.	.	PUNCT
eurjchem-170	235	20	biomed	biome	VERB
eurjchem-170	235	21	.	.	PUNCT
eurjchem-170	236	1	anal	anal	ADJ
eurjchem-170	236	2	.	.	PUNCT
eurjchem-170	237	1	2010	2010	NUM
eurjchem-170	237	2	,	,	PUNCT
eurjchem-170	237	3	51	51	NUM
eurjchem-170	237	4	,	,	PUNCT
eurjchem-170	237	5	1037‐	1037‐	NUM
eurjchem-170	237	6	1046	1046	NUM
eurjchem-170	237	7	.	.	PUNCT
eurjchem-170	238	1	[	[	X
eurjchem-170	238	2	8	8	NUM
eurjchem-170	238	3	]	]	PUNCT
eurjchem-170	238	4	.	.	PUNCT
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eurjchem-170	239	3	r.	r.	PROPN
eurjchem-170	239	4	p.	p.	PROPN
eurjchem-170	239	5	;	;	PUNCT
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eurjchem-170	239	8	s.	s.	PROPN
eurjchem-170	239	9	j.	j.	PROPN
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eurjchem-170	239	11	.	.	PUNCT
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eurjchem-170	239	13	.	.	PUNCT
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eurjchem-170	240	2	.	.	PUNCT
eurjchem-170	241	1	2010	2010	NUM
eurjchem-170	241	2	,	,	PUNCT
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eurjchem-170	241	4	,	,	PUNCT
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eurjchem-170	241	6	.	.	PUNCT
eurjchem-170	242	1	[	[	X
eurjchem-170	242	2	9	9	NUM
eurjchem-170	242	3	]	]	PUNCT
eurjchem-170	242	4	.	.	PUNCT
eurjchem-170	242	5	hoffman	hoffman	PROPN
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eurjchem-170	242	8	b.	b.	PROPN
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eurjchem-170	242	11	brunton	brunton	PROPN
eurjchem-170	242	12	,	,	PUNCT
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eurjchem-170	242	14	.	.	PROPN
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eurjchem-170	242	24	,	,	PUNCT
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eurjchem-170	242	29	,	,	PUNCT
eurjchem-170	242	30	859‐	859‐	NUM
eurjchem-170	242	31	860	860	NUM
eurjchem-170	242	32	,	,	PUNCT
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eurjchem-170	242	34	.	.	PUNCT
eurjchem-170	243	1	[	[	X
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eurjchem-170	243	3	]	]	PUNCT
eurjchem-170	243	4	.	.	PUNCT
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eurjchem-170	244	14	april	april	PROPN
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eurjchem-170	244	17	.	.	PUNCT
eurjchem-170	245	1	[	[	X
eurjchem-170	245	2	11	11	NUM
eurjchem-170	245	3	]	]	PUNCT
eurjchem-170	245	4	.	.	PUNCT
eurjchem-170	246	1	hsu	hsu	PROPN
eurjchem-170	246	2	,	,	PUNCT
eurjchem-170	246	3	l.	l.	PROPN
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eurjchem-170	246	6	liq	liq	PROPN
eurjchem-170	246	7	.	.	PUNCT
eurjchem-170	247	1	chrom	chrom	PROPN
eurjchem-170	247	2	.	.	PROPN
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eurjchem-170	247	5	.	.	PUNCT
eurjchem-170	248	1	technol	technol	PROPN
eurjchem-170	248	2	.	.	PROPN
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eurjchem-170	249	2	,	,	PUNCT
eurjchem-170	249	3	21	21	NUM
eurjchem-170	249	4	,	,	PUNCT
eurjchem-170	249	5	1685‐1700	1685‐1700	NUM
eurjchem-170	249	6	.	.	PUNCT
eurjchem-170	250	1	[	[	X
eurjchem-170	250	2	12	12	NUM
eurjchem-170	250	3	]	]	PUNCT
eurjchem-170	250	4	.	.	PUNCT
eurjchem-170	251	1	xue‐ning	xue‐ning	PROPN
eurjchem-170	251	2	,	,	PUNCT
eurjchem-170	251	3	l.	l.	PROPN
eurjchem-170	251	4	;	;	PUNCT
eurjchem-170	251	5	hong‐rong	hong‐rong	PROPN
eurjchem-170	251	6	,	,	PUNCT
eurjchem-170	251	7	x.	x.	NOUN
eurjchem-170	251	8	;	;	PUNCT
eurjchem-170	251	9	wei‐li	wei‐li	PROPN
eurjchem-170	251	10	,	,	PUNCT
eurjchem-170	251	11	c.	c.	PROPN
eurjchem-170	251	12	;	;	PUNCT
eurjchem-170	251	13	gang‐yi	gang‐yi	PROPN
eurjchem-170	251	14	,	,	PUNCT
eurjchem-170	251	15	l.	l.	PROPN
eurjchem-170	251	16	;	;	PUNCT
eurjchem-170	251	17	nan‐nan	nan‐nan	NUM
eurjchem-170	251	18	.	.	PUNCT
eurjchem-170	251	19	c.	c.	PROPN
eurjchem-170	251	20	;	;	PUNCT
eurjchem-170	251	21	chen	chen	PROPN
eurjchem-170	251	22	y.	y.	PROPN
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eurjchem-170	251	25	.	.	PUNCT
eurjchem-170	252	1	b	b	X
eurjchem-170	252	2	2007	2007	NUM
eurjchem-170	252	3	,	,	PUNCT
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eurjchem-170	252	5	,	,	PUNCT
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eurjchem-170	252	7	.	.	PUNCT
eurjchem-170	253	1	[	[	X
eurjchem-170	253	2	13	13	NUM
eurjchem-170	253	3	]	]	PUNCT
eurjchem-170	253	4	.	.	PUNCT
eurjchem-170	254	1	ferreirós	ferreirós	PROPN
eurjchem-170	254	2	,	,	PUNCT
eurjchem-170	254	3	n.	n.	NOUN
eurjchem-170	254	4	;	;	PUNCT
eurjchem-170	254	5	iriarte	iriarte	NOUN
eurjchem-170	254	6	,	,	PUNCT
eurjchem-170	254	7	g.	g.	PROPN
eurjchem-170	254	8	;	;	PUNCT
eurjchem-170	254	9	alonsoa	alonsoa	PROPN
eurjchem-170	254	10	,	,	PUNCT
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eurjchem-170	254	13	;	;	PUNCT
eurjchem-170	254	14	jiménez	jiménez	PROPN
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eurjchem-170	254	16	r.	r.	PROPN
eurjchem-170	254	17	m.	m.	PROPN
eurjchem-170	254	18	;	;	PUNCT
eurjchem-170	254	19	ortíz	ortíz	NOUN
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eurjchem-170	254	21	e.	e.	PROPN
eurjchem-170	254	22	j.	j.	PROPN
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eurjchem-170	254	24	.	.	PUNCT
eurjchem-170	255	1	a	a	DET
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eurjchem-170	255	3	,	,	PUNCT
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eurjchem-170	255	5	,	,	PUNCT
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eurjchem-170	255	7	.	.	PUNCT
eurjchem-170	256	1	[	[	X
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eurjchem-170	256	3	]	]	PUNCT
eurjchem-170	256	4	.	.	PUNCT
eurjchem-170	257	1	ich	ich	PROPN
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eurjchem-170	257	4	,	,	PUNCT
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eurjchem-170	257	7	:	:	PUNCT
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eurjchem-170	258	1	[	[	X
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eurjchem-170	258	3	]	]	SYM
eurjchem-170	258	4	.	.	PUNCT
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eurjchem-170	258	10	,	,	PUNCT
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eurjchem-170	258	12	j.	j.	PROPN
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eurjchem-170	259	2	.	.	PUNCT
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eurjchem-170	260	2	,	,	PUNCT
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eurjchem-170	260	4	,	,	PUNCT
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eurjchem-170	260	6	.	.	PUNCT
eurjchem-170	261	1	[	[	X
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eurjchem-170	261	3	]	]	PUNCT
eurjchem-170	261	4	.	.	PUNCT
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eurjchem-170	262	2	,	,	PUNCT
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eurjchem-170	262	4	;	;	PUNCT
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eurjchem-170	262	6	,	,	PUNCT
eurjchem-170	262	7	l.	l.	PROPN
eurjchem-170	262	8	;	;	PUNCT
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eurjchem-170	262	10	,	,	PUNCT
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eurjchem-170	263	2	.	.	PUNCT
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eurjchem-170	264	2	,	,	PUNCT
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eurjchem-170	264	12	.	.	PUNCT
eurjchem-170	265	1	[	[	X
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eurjchem-170	265	4	.	.	PUNCT
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eurjchem-170	266	3	g.	g.	PROPN
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eurjchem-170	266	5	;	;	PUNCT
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eurjchem-170	266	7	,	,	PUNCT
eurjchem-170	266	8	r.	r.	PROPN
eurjchem-170	266	9	;	;	PUNCT
eurjchem-170	266	10	ail	ail	X
eurjchem-170	266	11	,	,	PUNCT
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eurjchem-170	266	18	;	;	PUNCT
eurjchem-170	266	19	zhang	zhang	PROPN
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eurjchem-170	266	23	liu	liu	PROPN
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eurjchem-170	266	30	wang	wang	PROPN
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eurjchem-170	266	33	;	;	PUNCT
eurjchem-170	266	34	yang	yang	PROPN
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eurjchem-170	266	38	.	.	PUNCT
eurjchem-170	267	1	mass	mass	PROPN
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eurjchem-170	267	3	.	.	PUNCT
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eurjchem-170	268	2	,	,	PUNCT
eurjchem-170	268	3	23	23	NUM
eurjchem-170	268	4	,	,	PUNCT
eurjchem-170	268	5	425‐432	425‐432	NUM
eurjchem-170	268	6	.	.	PUNCT
eurjchem-170	269	1	[	[	X
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eurjchem-170	269	3	]	]	SYM
eurjchem-170	269	4	.	.	PUNCT
eurjchem-170	270	1	brum	brum	PROPN
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eurjchem-170	270	4	;	;	PUNCT
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eurjchem-170	270	6	,	,	PUNCT
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eurjchem-170	270	8	rapid	rapid	PROPN
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eurjchem-170	270	10	.	.	PUNCT
eurjchem-170	271	1	mass	mass	PROPN
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eurjchem-170	271	3	.	.	PUNCT
eurjchem-170	272	1	1997	1997	NUM
eurjchem-170	272	2	,	,	PUNCT
eurjchem-170	272	3	11	11	NUM
eurjchem-170	272	4	,	,	PUNCT
eurjchem-170	272	5	1430‐	1430‐	NUM
eurjchem-170	272	6	1434	1434	NUM
eurjchem-170	272	7	.	.	PUNCT
eurjchem-170	273	1	[	[	X
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eurjchem-170	273	3	]	]	PUNCT
eurjchem-170	273	4	.	.	PUNCT
eurjchem-170	273	5	thoma	thoma	PROPN
eurjchem-170	273	6	,	,	PUNCT
eurjchem-170	273	7	k.	k.	PROPN
eurjchem-170	273	8	;	;	PUNCT
eurjchem-170	273	9	kuebler	kuebler	PROPN
eurjchem-170	273	10	,	,	PUNCT
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eurjchem-170	273	12	;	;	PUNCT
eurjchem-170	273	13	reimann	reimann	PROPN
eurjchem-170	273	14	,	,	PUNCT
eurjchem-170	273	15	e.	e.	PROPN
eurjchem-170	273	16	pharmazie	pharmazie	PROPN
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eurjchem-170	273	18	,	,	PUNCT
eurjchem-170	273	19	52	52	NUM
eurjchem-170	273	20	,	,	PUNCT
eurjchem-170	273	21	362‐373	362‐373	NUM
eurjchem-170	273	22	.	.	PUNCT
eurjchem-170	274	1	[	[	X
eurjchem-170	274	2	20	20	NUM
eurjchem-170	274	3	]	]	PUNCT
eurjchem-170	274	4	.	.	PUNCT
eurjchem-170	274	5	albini	albini	PROPN
eurjchem-170	274	6	,	,	PUNCT
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eurjchem-170	274	8	;	;	PUNCT
eurjchem-170	274	9	fasani	fasani	PROPN
eurjchem-170	274	10	,	,	PUNCT
eurjchem-170	274	11	e.	e.	PROPN
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eurjchem-170	274	24	,	,	PUNCT
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eurjchem-170	274	27	,	,	PUNCT
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