id	sid	tid	token	lemma	pos
eurjchem-1700	1	1	quantitative	quantitative	ADJ
eurjchem-1700	1	2	determination	determination	NOUN
eurjchem-1700	1	3	of	of	ADP
eurjchem-1700	1	4	clobetasone	clobetasone	NOUN
eurjchem-1700	1	5	butyrate	butyrate	NOUN
eurjchem-1700	1	6	in	in	ADP
eurjchem-1700	1	7	bulk	bulk	ADJ
eurjchem-1700	1	8	and	and	CCONJ
eurjchem-1700	1	9	cream	cream	NOUN
eurjchem-1700	1	10	formulation	formulation	NOUN
eurjchem-1700	1	11	by	by	ADP
eurjchem-1700	1	12	a	a	DET
eurjchem-1700	1	13	validated	validate	VERB
eurjchem-1700	1	14	stability	stability	NOUN
eurjchem-1700	1	15	-	-	PUNCT
eurjchem-1700	1	16	indicating	indicate	VERB
eurjchem-1700	1	17	reversed	reverse	VERB
eurjchem-1700	1	18	-	-	PUNCT
eurjchem-1700	1	19	phase	phase	NOUN
eurjchem-1700	1	20	hplc	hplc	NOUN
eurjchem-1700	1	21	method	method	PROPN
eurjchem-1700	1	22	european	european	PROPN
eurjchem-1700	1	23	journal	journal	PROPN
eurjchem-1700	1	24	of	of	ADP
eurjchem-1700	1	25	chemistry	chemistry	NOUN
eurjchem-1700	1	26	9	9	NUM
eurjchem-1700	1	27	(	(	PUNCT
eurjchem-1700	1	28	2	2	NUM
eurjchem-1700	1	29	)	)	PUNCT
eurjchem-1700	1	30	(	(	PUNCT
eurjchem-1700	1	31	2018	2018	NUM
eurjchem-1700	1	32	)	)	PUNCT
eurjchem-1700	1	33	92	92	NUM
eurjchem-1700	1	34	-	-	SYM
eurjchem-1700	1	35	98	98	NUM
eurjchem-1700	1	36	european	european	ADJ
eurjchem-1700	1	37	journal	journal	NOUN
eurjchem-1700	1	38	of	of	ADP
eurjchem-1700	1	39	chemistry	chemistry	NOUN
eurjchem-1700	1	40	view	view	NOUN
eurjchem-1700	1	41	journal	journal	PROPN
eurjchem-1700	1	42	online	online	PROPN
eurjchem-1700	1	43	view	view	NOUN
eurjchem-1700	1	44	article	article	NOUN
eurjchem-1700	1	45	online	online	VERB
eurjchem-1700	1	46	quantitative	quantitative	ADJ
eurjchem-1700	1	47	determination	determination	NOUN
eurjchem-1700	1	48	of	of	ADP
eurjchem-1700	1	49	clobetasone	clobetasone	NOUN
eurjchem-1700	1	50	butyrate	butyrate	NOUN
eurjchem-1700	1	51	in	in	ADP
eurjchem-1700	1	52	bulk	bulk	ADJ
eurjchem-1700	1	53	and	and	CCONJ
eurjchem-1700	1	54	cream	cream	NOUN
eurjchem-1700	1	55	formulation	formulation	NOUN
eurjchem-1700	1	56	by	by	ADP
eurjchem-1700	1	57	a	a	DET
eurjchem-1700	1	58	validated	validate	VERB
eurjchem-1700	1	59	stability	stability	NOUN
eurjchem-1700	1	60	-	-	PUNCT
eurjchem-1700	1	61	indicating	indicate	VERB
eurjchem-1700	1	62	reversed	reverse	VERB
eurjchem-1700	1	63	-	-	PUNCT
eurjchem-1700	1	64	phase	phase	NOUN
eurjchem-1700	1	65	hplc	hplc	NOUN
eurjchem-1700	1	66	method	method	NOUN
eurjchem-1700	1	67	hassan	hassan	PROPN
eurjchem-1700	1	68	ahmad	ahmad	PROPN
eurjchem-1700	1	69	alhazmi	alhazmi	PROPN
eurjchem-1700	1	70	1,2	1,2	NUM
eurjchem-1700	1	71	,	,	PUNCT
eurjchem-1700	1	72	*	*	PUNCT
eurjchem-1700	1	73	,	,	PUNCT
eurjchem-1700	1	74	gunasekar	gunasekar	PROPN
eurjchem-1700	1	75	manoharan	manoharan	NOUN
eurjchem-1700	1	76	3	3	NUM
eurjchem-1700	1	77	,	,	PUNCT
eurjchem-1700	1	78	mohammed	mohammed	PROPN
eurjchem-1700	1	79	al	al	PROPN
eurjchem-1700	1	80	bratty	bratty	PROPN
eurjchem-1700	1	81	1	1	NUM
eurjchem-1700	1	82	and	and	CCONJ
eurjchem-1700	1	83	sadique	sadique	ADJ
eurjchem-1700	1	84	akhtar	akhtar	NOUN
eurjchem-1700	1	85	javed	javed	NOUN
eurjchem-1700	1	86	1	1	NUM
eurjchem-1700	1	87	1	1	NUM
eurjchem-1700	1	88	department	department	NOUN
eurjchem-1700	1	89	of	of	ADP
eurjchem-1700	1	90	pharmaceutical	pharmaceutical	ADJ
eurjchem-1700	1	91	chemistry	chemistry	NOUN
eurjchem-1700	1	92	,	,	PUNCT
eurjchem-1700	1	93	college	college	NOUN
eurjchem-1700	1	94	of	of	ADP
eurjchem-1700	1	95	pharmacy	pharmacy	NOUN
eurjchem-1700	1	96	,	,	PUNCT
eurjchem-1700	1	97	jazan	jazan	PROPN
eurjchem-1700	1	98	university	university	PROPN
eurjchem-1700	1	99	,	,	PUNCT
eurjchem-1700	1	100	jazan	jazan	NOUN
eurjchem-1700	1	101	,	,	PUNCT
eurjchem-1700	1	102	45142	45142	NUM
eurjchem-1700	1	103	,	,	PUNCT
eurjchem-1700	1	104	kingdom	kingdom	NOUN
eurjchem-1700	1	105	of	of	ADP
eurjchem-1700	1	106	saudi	saudi	PROPN
eurjchem-1700	1	107	arabia	arabia	PROPN
eurjchem-1700	1	108	haalhazmi@jazanu.edu.sa	haalhazmi@jazanu.edu.sa	PROPN
eurjchem-1700	1	109	(	(	PUNCT
eurjchem-1700	1	110	h.a.a	h.a.a	PROPN
eurjchem-1700	1	111	.	.	PUNCT
eurjchem-1700	1	112	)	)	PUNCT
eurjchem-1700	1	113	,	,	PUNCT
eurjchem-1700	1	114	malbratty@jazanu.edu.sa	malbratty@jazanu.edu.sa	PROPN
eurjchem-1700	1	115	(	(	PUNCT
eurjchem-1700	1	116	m.a	m.a	PROPN
eurjchem-1700	1	117	.	.	PROPN
eurjchem-1700	1	118	)	)	PUNCT
eurjchem-1700	1	119	,	,	PUNCT
eurjchem-1700	1	120	sajaved@jazanu.edu.sa	sajaved@jazanu.edu.sa	NOUN
eurjchem-1700	1	121	(	(	PUNCT
eurjchem-1700	1	122	s.a.j	s.a.j	ADJ
eurjchem-1700	1	123	.	.	PUNCT
eurjchem-1700	1	124	)	)	PUNCT
eurjchem-1700	2	1	2	2	NUM
eurjchem-1700	2	2	substance	substance	NOUN
eurjchem-1700	2	3	abuse	abuse	NOUN
eurjchem-1700	2	4	research	research	NOUN
eurjchem-1700	2	5	center	center	NOUN
eurjchem-1700	2	6	,	,	PUNCT
eurjchem-1700	2	7	jazan	jazan	PROPN
eurjchem-1700	2	8	university	university	PROPN
eurjchem-1700	2	9	,	,	PUNCT
eurjchem-1700	2	10	jazan	jazan	NOUN
eurjchem-1700	2	11	,	,	PUNCT
eurjchem-1700	2	12	45142	45142	NUM
eurjchem-1700	2	13	,	,	PUNCT
eurjchem-1700	2	14	kingdom	kingdom	NOUN
eurjchem-1700	2	15	of	of	ADP
eurjchem-1700	2	16	saudi	saudi	PROPN
eurjchem-1700	2	17	arabia	arabia	PROPN
eurjchem-1700	2	18	3	3	NUM
eurjchem-1700	2	19	chemistry	chemistry	NOUN
eurjchem-1700	2	20	department	department	NOUN
eurjchem-1700	2	21	,	,	PUNCT
eurjchem-1700	2	22	faculty	faculty	NOUN
eurjchem-1700	2	23	of	of	ADP
eurjchem-1700	2	24	science	science	NOUN
eurjchem-1700	2	25	,	,	PUNCT
eurjchem-1700	2	26	jazan	jazan	PROPN
eurjchem-1700	2	27	university	university	PROPN
eurjchem-1700	2	28	,	,	PUNCT
eurjchem-1700	2	29	jazan	jazan	NOUN
eurjchem-1700	2	30	,	,	PUNCT
eurjchem-1700	2	31	45142	45142	NUM
eurjchem-1700	2	32	,	,	PUNCT
eurjchem-1700	2	33	kingdom	kingdom	NOUN
eurjchem-1700	2	34	of	of	ADP
eurjchem-1700	2	35	saudi	saudi	PROPN
eurjchem-1700	2	36	arabia	arabia	PROPN
eurjchem-1700	2	37	shekarphd@yahoo.com	shekarphd@yahoo.com	PROPN
eurjchem-1700	2	38	(	(	PUNCT
eurjchem-1700	2	39	g.m	g.m	PROPN
eurjchem-1700	2	40	.	.	PUNCT
eurjchem-1700	2	41	)	)	PUNCT
eurjchem-1700	3	1	*	*	PUNCT
eurjchem-1700	3	2	corresponding	correspond	VERB
eurjchem-1700	3	3	author	author	NOUN
eurjchem-1700	3	4	at	at	ADP
eurjchem-1700	3	5	:	:	PUNCT
eurjchem-1700	3	6	department	department	NOUN
eurjchem-1700	3	7	of	of	ADP
eurjchem-1700	3	8	pharmaceutical	pharmaceutical	ADJ
eurjchem-1700	3	9	chemistry	chemistry	NOUN
eurjchem-1700	3	10	,	,	PUNCT
eurjchem-1700	3	11	college	college	NOUN
eurjchem-1700	3	12	of	of	ADP
eurjchem-1700	3	13	pharmacy	pharmacy	NOUN
eurjchem-1700	3	14	,	,	PUNCT
eurjchem-1700	3	15	jazan	jazan	PROPN
eurjchem-1700	3	16	university	university	PROPN
eurjchem-1700	3	17	,	,	PUNCT
eurjchem-1700	3	18	jazan	jazan	NOUN
eurjchem-1700	3	19	,	,	PUNCT
eurjchem-1700	3	20	45142	45142	NUM
eurjchem-1700	3	21	,	,	PUNCT
eurjchem-1700	3	22	kingdom	kingdom	NOUN
eurjchem-1700	3	23	of	of	ADP
eurjchem-1700	3	24	saudi	saudi	PROPN
eurjchem-1700	3	25	arabia	arabia	PROPN
eurjchem-1700	3	26	.	.	PUNCT
eurjchem-1700	4	1	tel	tel	ADP
eurjchem-1700	4	2	:	:	PUNCT
eurjchem-1700	4	3	+966.017.3342662	+966.017.3342662	PROPN
eurjchem-1700	4	4	fax	fax	PROPN
eurjchem-1700	4	5	:	:	PUNCT
eurjchem-1700	4	6	+966.017.3342662	+966.017.3342662	NUM
eurjchem-1700	4	7	e	e	NOUN
eurjchem-1700	4	8	-	-	NOUN
eurjchem-1700	4	9	mail	mail	NOUN
eurjchem-1700	4	10	:	:	PUNCT
eurjchem-1700	4	11	haalhazmi@jazanu.edu.sa	haalhazmi@jazanu.edu.sa	PROPN
eurjchem-1700	4	12	(	(	PUNCT
eurjchem-1700	4	13	h.a	h.a	PROPN
eurjchem-1700	4	14	.	.	PROPN
eurjchem-1700	4	15	alhazmi	alhazmi	PROPN
eurjchem-1700	4	16	)	)	PUNCT
eurjchem-1700	4	17	.	.	PUNCT
eurjchem-1700	5	1	10.5155	10.5155	NUM
eurjchem-1700	5	2	/	/	SYM
eurjchem-1700	5	3	eurjchem.9.2.92	eurjchem.9.2.92	NOUN
eurjchem-1700	5	4	-	-	PUNCT
eurjchem-1700	5	5	98.1700	98.1700	NUM
eurjchem-1700	5	6	received	receive	VERB
eurjchem-1700	5	7	:	:	PUNCT
eurjchem-1700	5	8	08	08	NUM
eurjchem-1700	5	9	march	march	PROPN
eurjchem-1700	5	10	2018	2018	NUM
eurjchem-1700	5	11	received	receive	VERB
eurjchem-1700	5	12	in	in	ADP
eurjchem-1700	5	13	revised	revise	VERB
eurjchem-1700	5	14	form	form	NOUN
eurjchem-1700	5	15	:	:	PUNCT
eurjchem-1700	5	16	11	11	NUM
eurjchem-1700	5	17	april	april	PROPN
eurjchem-1700	5	18	2018	2018	NUM
eurjchem-1700	5	19	accepted	accept	VERB
eurjchem-1700	5	20	:	:	PUNCT
eurjchem-1700	5	21	18	18	NUM
eurjchem-1700	5	22	april	april	PROPN
eurjchem-1700	5	23	2018	2018	NUM
eurjchem-1700	5	24	published	publish	VERB
eurjchem-1700	5	25	online	online	ADV
eurjchem-1700	5	26	:	:	PUNCT
eurjchem-1700	5	27	30	30	NUM
eurjchem-1700	5	28	june	june	PROPN
eurjchem-1700	5	29	2018	2018	NUM
eurjchem-1700	5	30	printed	print	VERB
eurjchem-1700	5	31	:	:	PUNCT
eurjchem-1700	5	32	30	30	NUM
eurjchem-1700	5	33	june	june	PROPN
eurjchem-1700	5	34	2018	2018	NUM
eurjchem-1700	5	35	a	a	DET
eurjchem-1700	5	36	simple	simple	ADJ
eurjchem-1700	5	37	isocratic	isocratic	ADJ
eurjchem-1700	5	38	reversed	reverse	VERB
eurjchem-1700	5	39	-	-	PUNCT
eurjchem-1700	5	40	phase	phase	NOUN
eurjchem-1700	5	41	hplc	hplc	NOUN
eurjchem-1700	5	42	method	method	NOUN
eurjchem-1700	5	43	for	for	ADP
eurjchem-1700	5	44	quantification	quantification	NOUN
eurjchem-1700	5	45	of	of	ADP
eurjchem-1700	5	46	clobetasone	clobetasone	NOUN
eurjchem-1700	5	47	in	in	ADP
eurjchem-1700	5	48	bulk	bulk	ADJ
eurjchem-1700	5	49	and	and	CCONJ
eurjchem-1700	5	50	cream	cream	NOUN
eurjchem-1700	5	51	dosage	dosage	NOUN
eurjchem-1700	5	52	forms	form	NOUN
eurjchem-1700	5	53	has	have	AUX
eurjchem-1700	5	54	been	be	AUX
eurjchem-1700	5	55	developed	develop	VERB
eurjchem-1700	5	56	.	.	PUNCT
eurjchem-1700	6	1	chromatographic	chromatographic	ADJ
eurjchem-1700	6	2	analysis	analysis	NOUN
eurjchem-1700	6	3	was	be	AUX
eurjchem-1700	6	4	accomplished	accomplish	VERB
eurjchem-1700	6	5	on	on	ADP
eurjchem-1700	6	6	an	an	DET
eurjchem-1700	6	7	c18	c18	NOUN
eurjchem-1700	6	8	column	column	NOUN
eurjchem-1700	6	9	utilizing	utilize	VERB
eurjchem-1700	6	10	a	a	DET
eurjchem-1700	6	11	mixture	mixture	NOUN
eurjchem-1700	6	12	of	of	ADP
eurjchem-1700	6	13	methanol	methanol	NOUN
eurjchem-1700	6	14	and	and	CCONJ
eurjchem-1700	6	15	water	water	NOUN
eurjchem-1700	6	16	(	(	PUNCT
eurjchem-1700	6	17	84:16	84:16	NUM
eurjchem-1700	6	18	v	v	NOUN
eurjchem-1700	6	19	:	:	PUNCT
eurjchem-1700	6	20	v	v	NOUN
eurjchem-1700	6	21	,	,	PUNCT
eurjchem-1700	6	22	ph	ph	NOUN
eurjchem-1700	6	23	=	=	NOUN
eurjchem-1700	6	24	6.0	6.0	NUM
eurjchem-1700	6	25	)	)	PUNCT
eurjchem-1700	6	26	as	as	ADP
eurjchem-1700	6	27	mobile	mobile	ADJ
eurjchem-1700	6	28	phase	phase	NOUN
eurjchem-1700	6	29	.	.	PUNCT
eurjchem-1700	7	1	an	an	DET
eurjchem-1700	7	2	effluent	effluent	ADJ
eurjchem-1700	7	3	flow	flow	NOUN
eurjchem-1700	7	4	rate	rate	NOUN
eurjchem-1700	7	5	of	of	ADP
eurjchem-1700	7	6	1	1	NUM
eurjchem-1700	7	7	ml	ml	NOUN
eurjchem-1700	7	8	/	/	SYM
eurjchem-1700	7	9	min	min	NOUN
eurjchem-1700	7	10	was	be	AUX
eurjchem-1700	7	11	adjusted	adjust	VERB
eurjchem-1700	7	12	and	and	CCONJ
eurjchem-1700	7	13	the	the	DET
eurjchem-1700	7	14	detection	detection	NOUN
eurjchem-1700	7	15	was	be	AUX
eurjchem-1700	7	16	made	make	VERB
eurjchem-1700	7	17	at	at	ADP
eurjchem-1700	7	18	240	240	NUM
eurjchem-1700	7	19	nm	nm	PRON
eurjchem-1700	7	20	wavelength	wavelength	NOUN
eurjchem-1700	7	21	.	.	PUNCT
eurjchem-1700	8	1	the	the	DET
eurjchem-1700	8	2	method	method	NOUN
eurjchem-1700	8	3	was	be	AUX
eurjchem-1700	8	4	evaluated	evaluate	VERB
eurjchem-1700	8	5	according	accord	VERB
eurjchem-1700	8	6	to	to	ADP
eurjchem-1700	8	7	ich	ich	PROPN
eurjchem-1700	8	8	guidelines	guideline	NOUN
eurjchem-1700	8	9	q2	q2	PROPN
eurjchem-1700	8	10	r1	r1	PROPN
eurjchem-1700	8	11	for	for	ADP
eurjchem-1700	8	12	linearity	linearity	NOUN
eurjchem-1700	8	13	,	,	PUNCT
eurjchem-1700	8	14	specificity	specificity	NOUN
eurjchem-1700	8	15	,	,	PUNCT
eurjchem-1700	8	16	sensitivity	sensitivity	NOUN
eurjchem-1700	8	17	,	,	PUNCT
eurjchem-1700	8	18	precision	precision	NOUN
eurjchem-1700	8	19	and	and	CCONJ
eurjchem-1700	8	20	accuracy	accuracy	NOUN
eurjchem-1700	8	21	.	.	PUNCT
eurjchem-1700	9	1	the	the	DET
eurjchem-1700	9	2	method	method	NOUN
eurjchem-1700	9	3	exhibited	exhibit	VERB
eurjchem-1700	9	4	good	good	ADJ
eurjchem-1700	9	5	linearity	linearity	NOUN
eurjchem-1700	9	6	with	with	ADP
eurjchem-1700	9	7	correlation	correlation	NOUN
eurjchem-1700	9	8	coefficient	coefficient	NOUN
eurjchem-1700	9	9	(	(	PUNCT
eurjchem-1700	9	10	r2	r2	PROPN
eurjchem-1700	9	11	)	)	PUNCT
eurjchem-1700	9	12	of	of	ADP
eurjchem-1700	9	13	0.9993	0.9993	NUM
eurjchem-1700	9	14	over	over	ADP
eurjchem-1700	9	15	the	the	DET
eurjchem-1700	9	16	concentration	concentration	NOUN
eurjchem-1700	9	17	range	range	NOUN
eurjchem-1700	9	18	from	from	ADP
eurjchem-1700	9	19	5	5	NUM
eurjchem-1700	9	20	to	to	PART
eurjchem-1700	9	21	50	50	NUM
eurjchem-1700	9	22	μg	μg	NOUN
eurjchem-1700	9	23	/	/	SYM
eurjchem-1700	9	24	ml	ml	PROPN
eurjchem-1700	9	25	.	.	PUNCT
eurjchem-1700	10	1	the	the	DET
eurjchem-1700	10	2	recoveries	recovery	NOUN
eurjchem-1700	10	3	of	of	ADP
eurjchem-1700	10	4	the	the	DET
eurjchem-1700	10	5	test	test	NOUN
eurjchem-1700	10	6	drug	drug	NOUN
eurjchem-1700	10	7	from	from	ADP
eurjchem-1700	10	8	the	the	DET
eurjchem-1700	10	9	cream	cream	NOUN
eurjchem-1700	10	10	sample	sample	NOUN
eurjchem-1700	10	11	was	be	AUX
eurjchem-1700	10	12	found	find	VERB
eurjchem-1700	10	13	to	to	PART
eurjchem-1700	10	14	be	be	AUX
eurjchem-1700	10	15	98.56	98.56	NUM
eurjchem-1700	10	16	to	to	ADP
eurjchem-1700	10	17	99.51	99.51	NUM
eurjchem-1700	10	18	%	%	NOUN
eurjchem-1700	10	19	and	and	CCONJ
eurjchem-1700	10	20	the	the	DET
eurjchem-1700	10	21	limit	limit	NOUN
eurjchem-1700	10	22	of	of	ADP
eurjchem-1700	10	23	detection	detection	NOUN
eurjchem-1700	10	24	and	and	CCONJ
eurjchem-1700	10	25	quantification	quantification	NOUN
eurjchem-1700	10	26	were	be	AUX
eurjchem-1700	10	27	calculated	calculate	VERB
eurjchem-1700	10	28	as	as	ADP
eurjchem-1700	10	29	0.85	0.85	NUM
eurjchem-1700	10	30	and	and	CCONJ
eurjchem-1700	10	31	2.83	2.83	NUM
eurjchem-1700	10	32	μg	μg	PROPN
eurjchem-1700	10	33	/	/	SYM
eurjchem-1700	10	34	ml	ml	NOUN
eurjchem-1700	10	35	,	,	PUNCT
eurjchem-1700	10	36	respectively	respectively	ADV
eurjchem-1700	10	37	,	,	PUNCT
eurjchem-1700	10	38	suggesting	suggest	VERB
eurjchem-1700	10	39	the	the	DET
eurjchem-1700	10	40	accuracy	accuracy	NOUN
eurjchem-1700	10	41	and	and	CCONJ
eurjchem-1700	10	42	sensitivity	sensitivity	NOUN
eurjchem-1700	10	43	of	of	ADP
eurjchem-1700	10	44	the	the	DET
eurjchem-1700	10	45	developed	develop	VERB
eurjchem-1700	10	46	method	method	NOUN
eurjchem-1700	10	47	.	.	PUNCT
eurjchem-1700	11	1	the	the	DET
eurjchem-1700	11	2	precision	precision	NOUN
eurjchem-1700	11	3	was	be	AUX
eurjchem-1700	11	4	demonstrated	demonstrate	VERB
eurjchem-1700	11	5	by	by	ADP
eurjchem-1700	11	6	a	a	DET
eurjchem-1700	11	7	low	low	ADJ
eurjchem-1700	11	8	percentage	percentage	NOUN
eurjchem-1700	11	9	of	of	ADP
eurjchem-1700	11	10	relative	relative	ADJ
eurjchem-1700	11	11	standard	standard	ADJ
eurjchem-1700	11	12	deviation	deviation	NOUN
eurjchem-1700	11	13	(	(	PUNCT
eurjchem-1700	11	14	<	<	NOUN
eurjchem-1700	11	15	1	1	NUM
eurjchem-1700	11	16	%	%	NOUN
eurjchem-1700	11	17	)	)	PUNCT
eurjchem-1700	11	18	from	from	ADP
eurjchem-1700	11	19	six	six	NUM
eurjchem-1700	11	20	independent	independent	ADJ
eurjchem-1700	11	21	assay	assay	NOUN
eurjchem-1700	11	22	analysis	analysis	NOUN
eurjchem-1700	11	23	performed	perform	VERB
eurjchem-1700	11	24	for	for	ADP
eurjchem-1700	11	25	the	the	DET
eurjchem-1700	11	26	cream	cream	NOUN
eurjchem-1700	11	27	formulation	formulation	NOUN
eurjchem-1700	11	28	.	.	PUNCT
eurjchem-1700	12	1	stability	stability	NOUN
eurjchem-1700	12	2	indicating	indicate	VERB
eurjchem-1700	12	3	property	property	NOUN
eurjchem-1700	12	4	of	of	ADP
eurjchem-1700	12	5	the	the	DET
eurjchem-1700	12	6	proposed	propose	VERB
eurjchem-1700	12	7	method	method	NOUN
eurjchem-1700	12	8	was	be	AUX
eurjchem-1700	12	9	demonstrated	demonstrate	VERB
eurjchem-1700	12	10	by	by	ADP
eurjchem-1700	12	11	performing	perform	VERB
eurjchem-1700	12	12	the	the	DET
eurjchem-1700	12	13	analysis	analysis	NOUN
eurjchem-1700	12	14	of	of	ADP
eurjchem-1700	12	15	forced	force	VERB
eurjchem-1700	12	16	degradation	degradation	NOUN
eurjchem-1700	12	17	samples	sample	NOUN
eurjchem-1700	12	18	.	.	PUNCT
eurjchem-1700	13	1	the	the	DET
eurjchem-1700	13	2	developed	develop	VERB
eurjchem-1700	13	3	method	method	NOUN
eurjchem-1700	13	4	can	can	AUX
eurjchem-1700	13	5	be	be	AUX
eurjchem-1700	13	6	used	use	VERB
eurjchem-1700	13	7	for	for	ADP
eurjchem-1700	13	8	estimation	estimation	NOUN
eurjchem-1700	13	9	of	of	ADP
eurjchem-1700	13	10	the	the	DET
eurjchem-1700	13	11	clobetasone	clobetasone	NOUN
eurjchem-1700	13	12	butyrate	butyrate	NOUN
eurjchem-1700	13	13	in	in	ADP
eurjchem-1700	13	14	bulk	bulk	ADJ
eurjchem-1700	13	15	and	and	CCONJ
eurjchem-1700	13	16	pharmaceutical	pharmaceutical	NOUN
eurjchem-1700	13	17	formulations	formulation	NOUN
eurjchem-1700	13	18	for	for	ADP
eurjchem-1700	13	19	routine	routine	ADJ
eurjchem-1700	13	20	analysis	analysis	NOUN
eurjchem-1700	13	21	in	in	ADP
eurjchem-1700	13	22	the	the	DET
eurjchem-1700	13	23	quality	quality	NOUN
eurjchem-1700	13	24	control	control	NOUN
eurjchem-1700	13	25	laboratories	laboratory	NOUN
eurjchem-1700	13	26	.	.	PUNCT
eurjchem-1700	14	1	degradation	degradation	NOUN
eurjchem-1700	14	2	hplc	hplc	NOUN
eurjchem-1700	14	3	method	method	NOUN
eurjchem-1700	14	4	reversed	reverse	VERB
eurjchem-1700	14	5	-	-	PUNCT
eurjchem-1700	14	6	phase	phase	NOUN
eurjchem-1700	14	7	cream	cream	NOUN
eurjchem-1700	14	8	formulation	formulation	NOUN
eurjchem-1700	14	9	stability	stability	NOUN
eurjchem-1700	14	10	-	-	PUNCT
eurjchem-1700	14	11	indicating	indicate	VERB
eurjchem-1700	14	12	clobetasone	clobetasone	NOUN
eurjchem-1700	14	13	butyrate	butyrate	NOUN
eurjchem-1700	14	14	cite	cite	VERB
eurjchem-1700	14	15	this	this	PRON
eurjchem-1700	14	16	:	:	PUNCT
eurjchem-1700	14	17	eur	eur	PROPN
eurjchem-1700	14	18	.	.	PUNCT
eurjchem-1700	15	1	j.	j.	PROPN
eurjchem-1700	15	2	chem	chem	PROPN
eurjchem-1700	15	3	.	.	PUNCT
eurjchem-1700	16	1	2018	2018	NUM
eurjchem-1700	16	2	,	,	PUNCT
eurjchem-1700	16	3	9(2	9(2	NUM
eurjchem-1700	16	4	)	)	PUNCT
eurjchem-1700	16	5	,	,	PUNCT
eurjchem-1700	16	6	92	92	NUM
eurjchem-1700	16	7	-	-	SYM
eurjchem-1700	16	8	98	98	NUM
eurjchem-1700	16	9	journal	journal	NOUN
eurjchem-1700	16	10	website	website	NOUN
eurjchem-1700	16	11	:	:	PUNCT
eurjchem-1700	16	12	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1700	16	13	1	1	X
eurjchem-1700	16	14	.	.	PUNCT
eurjchem-1700	16	15	introduction	introduction	NOUN
eurjchem-1700	16	16	clobetasone	clobetasone	NOUN
eurjchem-1700	16	17	butyrate	butyrate	NOUN
eurjchem-1700	16	18	is	be	AUX
eurjchem-1700	16	19	chemically	chemically	ADV
eurjchem-1700	16	20	,	,	PUNCT
eurjchem-1700	16	21	21	21	NUM
eurjchem-1700	16	22	-	-	PUNCT
eurjchem-1700	16	23	chloro-9	chloro-9	PRON
eurjchem-1700	16	24	-	-	PUNCT
eurjchem-1700	16	25	fluoro-17hydroxy-16b	fluoro-17hydroxy-16b	NOUN
eurjchem-1700	16	26	-	-	PUNCT
eurjchem-1700	16	27	methylpregna-1,4	methylpregna-1,4	PROPN
eurjchem-1700	16	28	-	-	PUNCT
eurjchem-1700	16	29	diene-3,11,20	diene-3,11,20	VERB
eurjchem-1700	16	30	-	-	ADJ
eurjchem-1700	16	31	trione-17	trione-17	NOUN
eurjchem-1700	16	32	-	-	PUNCT
eurjchem-1700	16	33	butyrate	butyrate	NOUN
eurjchem-1700	16	34	(	(	PUNCT
eurjchem-1700	16	35	figure	figure	NOUN
eurjchem-1700	16	36	1	1	NUM
eurjchem-1700	16	37	)	)	PUNCT
eurjchem-1700	16	38	,	,	PUNCT
eurjchem-1700	16	39	a	a	DET
eurjchem-1700	16	40	potent	potent	ADJ
eurjchem-1700	16	41	corticosteroid	corticosteroid	NOUN
eurjchem-1700	16	42	and	and	CCONJ
eurjchem-1700	16	43	as	as	ADP
eurjchem-1700	16	44	butyrate	butyrate	ADJ
eurjchem-1700	16	45	ester	ester	NOUN
eurjchem-1700	16	46	,	,	PUNCT
eurjchem-1700	16	47	it	it	PRON
eurjchem-1700	16	48	is	be	AUX
eurjchem-1700	16	49	used	use	VERB
eurjchem-1700	16	50	topically	topically	ADV
eurjchem-1700	16	51	for	for	ADP
eurjchem-1700	16	52	the	the	DET
eurjchem-1700	16	53	treatment	treatment	NOUN
eurjchem-1700	16	54	of	of	ADP
eurjchem-1700	16	55	skin	skin	NOUN
eurjchem-1700	16	56	inflammation	inflammation	NOUN
eurjchem-1700	16	57	associated	associate	VERB
eurjchem-1700	16	58	with	with	ADP
eurjchem-1700	16	59	psoriasis	psoriasis	NOUN
eurjchem-1700	16	60	,	,	PUNCT
eurjchem-1700	16	61	eczema	eczema	NOUN
eurjchem-1700	16	62	and	and	CCONJ
eurjchem-1700	16	63	other	other	ADJ
eurjchem-1700	16	64	dermatitis	dermatitis	NOUN
eurjchem-1700	16	65	forms	form	NOUN
eurjchem-1700	16	66	[	[	X
eurjchem-1700	16	67	1	1	NUM
eurjchem-1700	16	68	-	-	SYM
eurjchem-1700	16	69	3	3	NUM
eurjchem-1700	16	70	]	]	PUNCT
eurjchem-1700	16	71	.	.	PUNCT
eurjchem-1700	17	1	it	it	PRON
eurjchem-1700	17	2	is	be	AUX
eurjchem-1700	17	3	not	not	PART
eurjchem-1700	17	4	a	a	DET
eurjchem-1700	17	5	cure	cure	NOUN
eurjchem-1700	17	6	for	for	ADP
eurjchem-1700	17	7	the	the	DET
eurjchem-1700	17	8	condition	condition	NOUN
eurjchem-1700	17	9	,	,	PUNCT
eurjchem-1700	17	10	but	but	CCONJ
eurjchem-1700	17	11	helps	help	VERB
eurjchem-1700	17	12	to	to	PART
eurjchem-1700	17	13	relieve	relieve	VERB
eurjchem-1700	17	14	the	the	DET
eurjchem-1700	17	15	symptoms	symptom	NOUN
eurjchem-1700	17	16	.	.	PUNCT
eurjchem-1700	18	1	although	although	SCONJ
eurjchem-1700	18	2	less	less	ADV
eurjchem-1700	18	3	potent	potent	ADJ
eurjchem-1700	18	4	topical	topical	ADJ
eurjchem-1700	18	5	steroids	steroid	NOUN
eurjchem-1700	18	6	are	be	AUX
eurjchem-1700	18	7	often	often	ADV
eurjchem-1700	18	8	preferred	prefer	VERB
eurjchem-1700	18	9	for	for	ADP
eurjchem-1700	18	10	use	use	NOUN
eurjchem-1700	18	11	in	in	ADP
eurjchem-1700	18	12	children	child	NOUN
eurjchem-1700	18	13	.	.	PUNCT
eurjchem-1700	19	1	a	a	DET
eurjchem-1700	19	2	short	short	ADJ
eurjchem-1700	19	3	course	course	NOUN
eurjchem-1700	19	4	of	of	ADP
eurjchem-1700	19	5	clobetasone	clobetasone	NOUN
eurjchem-1700	19	6	butyrate	butyrate	NOUN
eurjchem-1700	19	7	may	may	AUX
eurjchem-1700	19	8	be	be	AUX
eurjchem-1700	19	9	prescribed	prescribe	VERB
eurjchem-1700	19	10	for	for	ADP
eurjchem-1700	19	11	children	child	NOUN
eurjchem-1700	19	12	with	with	ADP
eurjchem-1700	19	13	severe	severe	ADJ
eurjchem-1700	19	14	eczema	eczema	NOUN
eurjchem-1700	19	15	on	on	ADP
eurjchem-1700	19	16	the	the	DET
eurjchem-1700	19	17	arms	arm	NOUN
eurjchem-1700	19	18	or	or	CCONJ
eurjchem-1700	19	19	legs	leg	NOUN
eurjchem-1700	19	20	.	.	PUNCT
eurjchem-1700	20	1	clobetasone	clobetasone	NOUN
eurjchem-1700	20	2	butyrate	butyrate	NOUN
eurjchem-1700	20	3	may	may	AUX
eurjchem-1700	20	4	also	also	ADV
eurjchem-1700	20	5	be	be	AUX
eurjchem-1700	20	6	prescribed	prescribe	VERB
eurjchem-1700	20	7	for	for	ADP
eurjchem-1700	20	8	the	the	DET
eurjchem-1700	20	9	short	short	ADJ
eurjchem-1700	20	10	courses	course	NOUN
eurjchem-1700	20	11	treatment	treatment	NOUN
eurjchem-1700	20	12	of	of	ADP
eurjchem-1700	20	13	psoriasis	psoriasis	NOUN
eurjchem-1700	20	14	for	for	ADP
eurjchem-1700	20	15	areas	area	NOUN
eurjchem-1700	20	16	like	like	ADP
eurjchem-1700	20	17	face	face	NOUN
eurjchem-1700	20	18	or	or	CCONJ
eurjchem-1700	20	19	inside	inside	ADP
eurjchem-1700	20	20	of	of	ADP
eurjchem-1700	20	21	elbows	elbow	NOUN
eurjchem-1700	20	22	and	and	CCONJ
eurjchem-1700	20	23	knees	knee	NOUN
eurjchem-1700	21	1	[	[	X
eurjchem-1700	21	2	4	4	NUM
eurjchem-1700	21	3	]	]	PUNCT
eurjchem-1700	21	4	.	.	PUNCT
eurjchem-1700	22	1	clobetasone	clobetasone	NOUN
eurjchem-1700	22	2	butyrate	butyrate	NOUN
eurjchem-1700	22	3	(	(	PUNCT
eurjchem-1700	22	4	0.05	0.05	NUM
eurjchem-1700	22	5	%	%	NOUN
eurjchem-1700	22	6	)	)	PUNCT
eurjchem-1700	22	7	cream	cream	NOUN
eurjchem-1700	22	8	formulation	formulation	NOUN
eurjchem-1700	22	9	,	,	PUNCT
eurjchem-1700	22	10	classified	classify	VERB
eurjchem-1700	22	11	as	as	ADP
eurjchem-1700	22	12	otc	otc	PROPN
eurjchem-1700	22	13	(	(	PUNCT
eurjchem-1700	22	14	over	over	ADP
eurjchem-1700	22	15	the	the	DET
eurjchem-1700	22	16	counter	counter	NOUN
eurjchem-1700	22	17	)	)	PUNCT
eurjchem-1700	22	18	product	product	NOUN
eurjchem-1700	22	19	,	,	PUNCT
eurjchem-1700	22	20	has	have	AUX
eurjchem-1700	22	21	been	be	AUX
eurjchem-1700	22	22	available	available	ADJ
eurjchem-1700	22	23	in	in	ADP
eurjchem-1700	22	24	the	the	DET
eurjchem-1700	22	25	pharmacy	pharmacy	NOUN
eurjchem-1700	22	26	stores	store	NOUN
eurjchem-1700	22	27	and	and	CCONJ
eurjchem-1700	22	28	used	use	VERB
eurjchem-1700	22	29	to	to	PART
eurjchem-1700	22	30	treat	treat	VERB
eurjchem-1700	22	31	mainly	mainly	ADV
eurjchem-1700	22	32	acute	acute	ADJ
eurjchem-1700	22	33	eczema	eczema	NOUN
eurjchem-1700	22	34	and	and	CCONJ
eurjchem-1700	22	35	allergic	allergic	ADJ
eurjchem-1700	22	36	dermatitis	dermatitis	NOUN
eurjchem-1700	22	37	in	in	ADP
eurjchem-1700	22	38	both	both	DET
eurjchem-1700	22	39	adults	adult	NOUN
eurjchem-1700	22	40	and	and	CCONJ
eurjchem-1700	22	41	children	child	NOUN
eurjchem-1700	22	42	.	.	PUNCT
eurjchem-1700	23	1	comparative	comparative	ADJ
eurjchem-1700	23	2	studies	study	NOUN
eurjchem-1700	23	3	have	have	AUX
eurjchem-1700	23	4	reported	report	VERB
eurjchem-1700	23	5	that	that	SCONJ
eurjchem-1700	23	6	clobetasone	clobetasone	NOUN
eurjchem-1700	23	7	butyrate	butyrate	NOUN
eurjchem-1700	23	8	(	(	PUNCT
eurjchem-1700	23	9	0.05	0.05	NUM
eurjchem-1700	23	10	%	%	NOUN
eurjchem-1700	23	11	)	)	PUNCT
eurjchem-1700	23	12	was	be	AUX
eurjchem-1700	23	13	more	more	ADV
eurjchem-1700	23	14	effective	effective	ADJ
eurjchem-1700	23	15	than	than	ADP
eurjchem-1700	23	16	other	other	ADJ
eurjchem-1700	23	17	topical	topical	ADJ
eurjchem-1700	23	18	steroids	steroid	NOUN
eurjchem-1700	23	19	such	such	ADJ
eurjchem-1700	23	20	as	as	ADP
eurjchem-1700	23	21	hydrocortisone	hydrocortisone	PROPN
eurjchem-1700	23	22	butyrate	butyrate	NOUN
eurjchem-1700	23	23	(	(	PUNCT
eurjchem-1700	23	24	1.0	1.0	NUM
eurjchem-1700	23	25	%	%	NOUN
eurjchem-1700	23	26	)	)	PUNCT
eurjchem-1700	23	27	and	and	CCONJ
eurjchem-1700	23	28	flurandrelone	flurandrelone	NOUN
eurjchem-1700	23	29	(	(	PUNCT
eurjchem-1700	23	30	0.0125	0.0125	NUM
eurjchem-1700	23	31	%	%	NOUN
eurjchem-1700	23	32	)	)	PUNCT
eurjchem-1700	23	33	for	for	ADP
eurjchem-1700	23	34	the	the	DET
eurjchem-1700	23	35	treatment	treatment	NOUN
eurjchem-1700	23	36	skin	skin	NOUN
eurjchem-1700	23	37	inflammatory	inflammatory	ADJ
eurjchem-1700	23	38	conditions	condition	NOUN
eurjchem-1700	23	39	.	.	PUNCT
eurjchem-1700	24	1	additionally	additionally	ADV
eurjchem-1700	24	2	,	,	PUNCT
eurjchem-1700	24	3	due	due	ADP
eurjchem-1700	24	4	to	to	ADP
eurjchem-1700	24	5	negligible	negligible	ADJ
eurjchem-1700	24	6	systemic	systemic	ADJ
eurjchem-1700	24	7	absorption	absorption	NOUN
eurjchem-1700	24	8	,	,	PUNCT
eurjchem-1700	24	9	it	it	PRON
eurjchem-1700	24	10	has	have	AUX
eurjchem-1700	24	11	been	be	AUX
eurjchem-1700	24	12	considered	consider	VERB
eurjchem-1700	24	13	to	to	PART
eurjchem-1700	24	14	be	be	AUX
eurjchem-1700	24	15	systemically	systemically	ADV
eurjchem-1700	24	16	safe	safe	ADJ
eurjchem-1700	24	17	[	[	X
eurjchem-1700	24	18	5,6	5,6	NUM
eurjchem-1700	24	19	]	]	PUNCT
eurjchem-1700	24	20	.	.	PUNCT
eurjchem-1700	25	1	apart	apart	ADV
eurjchem-1700	25	2	from	from	ADP
eurjchem-1700	25	3	dermal	dermal	ADJ
eurjchem-1700	25	4	conditions	condition	NOUN
eurjchem-1700	25	5	,	,	PUNCT
eurjchem-1700	25	6	clobetasone	clobetasone	NOUN
eurjchem-1700	25	7	butyrate	butyrate	NOUN
eurjchem-1700	25	8	has	have	AUX
eurjchem-1700	25	9	also	also	ADV
eurjchem-1700	25	10	found	find	VERB
eurjchem-1700	25	11	its	its	PRON
eurjchem-1700	25	12	application	application	NOUN
eurjchem-1700	25	13	in	in	ADP
eurjchem-1700	25	14	ophthalmic	ophthalmic	ADJ
eurjchem-1700	25	15	inflammatory	inflammatory	ADJ
eurjchem-1700	25	16	conditions	condition	NOUN
eurjchem-1700	25	17	,	,	PUNCT
eurjchem-1700	25	18	where	where	SCONJ
eurjchem-1700	25	19	it	it	PRON
eurjchem-1700	25	20	is	be	AUX
eurjchem-1700	25	21	applied	apply	VERB
eurjchem-1700	25	22	as	as	ADP
eurjchem-1700	25	23	1.0	1.0	NUM
eurjchem-1700	25	24	%	%	NOUN
eurjchem-1700	25	25	clobetasone	clobetasone	NOUN
eurjchem-1700	25	26	butyrate	butyrate	NOUN
eurjchem-1700	25	27	eye	eye	NOUN
eurjchem-1700	25	28	drop	drop	NOUN
eurjchem-1700	25	29	[	[	X
eurjchem-1700	25	30	2,7	2,7	NUM
eurjchem-1700	25	31	]	]	PUNCT
eurjchem-1700	25	32	.	.	PUNCT
eurjchem-1700	26	1	o	o	X
eurjchem-1700	27	1	f	f	X
eurjchem-1700	28	1	o	o	X
eurjchem-1700	29	1	o	o	X
eurjchem-1700	29	2	cl	cl	INTJ
eurjchem-1700	30	1	o	o	NOUN
eurjchem-1700	30	2	h3c	h3c	PUNCT
eurjchem-1700	30	3	o	o	NOUN
eurjchem-1700	30	4	figure	figure	NOUN
eurjchem-1700	30	5	1	1	NUM
eurjchem-1700	30	6	.	.	PUNCT
eurjchem-1700	30	7	chemical	chemical	ADJ
eurjchem-1700	30	8	structure	structure	NOUN
eurjchem-1700	30	9	of	of	ADP
eurjchem-1700	30	10	clobetasone	clobetasone	NOUN
eurjchem-1700	30	11	butyrate	butyrate	NOUN
eurjchem-1700	30	12	.	.	PUNCT
eurjchem-1700	31	1	abstract	abstract	ADJ
eurjchem-1700	31	2	research	research	NOUN
eurjchem-1700	31	3	article	article	NOUN
eurjchem-1700	31	4	keywords	keyword	VERB
eurjchem-1700	31	5	european	european	PROPN
eurjchem-1700	31	6	journal	journal	PROPN
eurjchem-1700	31	7	of	of	ADP
eurjchem-1700	31	8	chemistry	chemistry	NOUN
eurjchem-1700	31	9	issn	issn	VERB
eurjchem-1700	31	10	2153	2153	NUM
eurjchem-1700	31	11	-	-	SYM
eurjchem-1700	31	12	2249	2249	NUM
eurjchem-1700	31	13	(	(	PUNCT
eurjchem-1700	31	14	print	print	NOUN
eurjchem-1700	31	15	)	)	PUNCT
eurjchem-1700	31	16	/	/	PUNCT
eurjchem-1700	31	17	issn	issn	PROPN
eurjchem-1700	31	18	2153	2153	NUM
eurjchem-1700	31	19	-	-	SYM
eurjchem-1700	31	20	2257	2257	NUM
eurjchem-1700	31	21	(	(	PUNCT
eurjchem-1700	31	22	online	online	ADJ
eurjchem-1700	31	23	)	)	PUNCT
eurjchem-1700	31	24	–	–	PUNCT
eurjchem-1700	32	1	copyright	copyright	NOUN
eurjchem-1700	32	2	©	©	PROPN
eurjchem-1700	32	3	2018	2018	NUM
eurjchem-1700	32	4	the	the	DET
eurjchem-1700	32	5	authors	author	NOUN
eurjchem-1700	32	6	–	–	PUNCT
eurjchem-1700	32	7	atlanta	atlanta	PROPN
eurjchem-1700	32	8	publishing	publishing	PROPN
eurjchem-1700	32	9	house	house	PROPN
eurjchem-1700	32	10	llc	llc	PROPN
eurjchem-1700	32	11	–	–	PUNCT
eurjchem-1700	32	12	printed	print	VERB
eurjchem-1700	32	13	in	in	ADP
eurjchem-1700	32	14	the	the	DET
eurjchem-1700	32	15	usa	usa	PROPN
eurjchem-1700	32	16	.	.	PUNCT
eurjchem-1700	33	1	this	this	DET
eurjchem-1700	33	2	work	work	NOUN
eurjchem-1700	33	3	is	be	AUX
eurjchem-1700	33	4	published	publish	VERB
eurjchem-1700	33	5	and	and	CCONJ
eurjchem-1700	33	6	licensed	license	VERB
eurjchem-1700	33	7	by	by	ADP
eurjchem-1700	33	8	atlanta	atlanta	PROPN
eurjchem-1700	33	9	publishing	publishing	PROPN
eurjchem-1700	33	10	house	house	PROPN
eurjchem-1700	33	11	llc	llc	PROPN
eurjchem-1700	33	12	–	–	PUNCT
eurjchem-1700	33	13	cc	cc	PROPN
eurjchem-1700	33	14	by	by	ADP
eurjchem-1700	33	15	nc	nc	PROPN
eurjchem-1700	33	16	–	–	PUNCT
eurjchem-1700	33	17	some	some	DET
eurjchem-1700	33	18	rights	right	NOUN
eurjchem-1700	33	19	reserved	reserve	VERB
eurjchem-1700	33	20	.	.	PUNCT
eurjchem-1700	34	1	http://dx.doi.org/10.5155/eurjchem.9.2.92-98.1700	http://dx.doi.org/10.5155/eurjchem.9.2.92-98.1700	NOUN
eurjchem-1700	34	2	http://dx.doi.org/10.5155/eurjchem.9.2.92-98.1700	http://dx.doi.org/10.5155/eurjchem.9.2.92-98.1700	PROPN
eurjchem-1700	34	3	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.9.2.92-98.1700&domain=pdf&date_stamp=2018-06-30	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.9.2.92-98.1700&domain=pdf&date_stamp=2018-06-30	NOUN
eurjchem-1700	34	4	http://www.eurjchem.com/	http://www.eurjchem.com/	NOUN
eurjchem-1700	34	5	http://dx.doi.org/10.5155/eurjchem.9.2.92-98.1700	http://dx.doi.org/10.5155/eurjchem.9.2.92-98.1700	NUM
eurjchem-1700	34	6	mailto:haalhazmi@jazanu.edu.sa	mailto:haalhazmi@jazanu.edu.sa	PROPN
eurjchem-1700	34	7	mailto:malbratty@jazanu.edu.sa	mailto:malbratty@jazanu.edu.sa	PROPN
eurjchem-1700	34	8	mailto:sajaved@jazanu.edu.sa	mailto:sajaved@jazanu.edu.sa	PROPN
eurjchem-1700	34	9	mailto:shekarphd@yahoo.com	mailto:shekarphd@yahoo.com	PROPN
eurjchem-1700	35	1	mailto:haalhazmi@jazanu.edu.sa	mailto:haalhazmi@jazanu.edu.sa	PROPN
eurjchem-1700	35	2	http://www.eurjchem.com/	http://www.eurjchem.com/	PROPN
eurjchem-1700	35	3	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.9.2.92-98.1700&domain=pdf&date_stamp=2018-06-30	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.9.2.92-98.1700&domain=pdf&date_stamp=2018-06-30	PROPN
eurjchem-1700	35	4	�	�	PROPN
eurjchem-1700	35	5	alhazmi	alhazmi	PROPN
eurjchem-1700	35	6	et	et	PROPN
eurjchem-1700	35	7	al	al	PROPN
eurjchem-1700	35	8	.	.	PUNCT
eurjchem-1700	35	9	/	/	SYM
eurjchem-1700	35	10	european	european	PROPN
eurjchem-1700	35	11	journal	journal	PROPN
eurjchem-1700	35	12	of	of	ADP
eurjchem-1700	35	13	chemistry	chemistry	NOUN
eurjchem-1700	35	14	9	9	NUM
eurjchem-1700	35	15	(	(	PUNCT
eurjchem-1700	35	16	2	2	NUM
eurjchem-1700	35	17	)	)	PUNCT
eurjchem-1700	35	18	(	(	PUNCT
eurjchem-1700	35	19	2018	2018	NUM
eurjchem-1700	35	20	)	)	PUNCT
eurjchem-1700	35	21	92	92	NUM
eurjchem-1700	35	22	-	-	SYM
eurjchem-1700	35	23	98	98	NUM
eurjchem-1700	35	24	93	93	NUM
eurjchem-1700	35	25	an	an	DET
eurjchem-1700	35	26	extensive	extensive	ADJ
eurjchem-1700	35	27	literature	literature	NOUN
eurjchem-1700	35	28	survey	survey	NOUN
eurjchem-1700	35	29	revealed	reveal	VERB
eurjchem-1700	35	30	that	that	SCONJ
eurjchem-1700	35	31	,	,	PUNCT
eurjchem-1700	35	32	an	an	DET
eurjchem-1700	35	33	insignificant	insignificant	ADJ
eurjchem-1700	35	34	amount	amount	NOUN
eurjchem-1700	35	35	of	of	ADP
eurjchem-1700	35	36	attention	attention	NOUN
eurjchem-1700	35	37	has	have	AUX
eurjchem-1700	35	38	been	be	AUX
eurjchem-1700	35	39	paid	pay	VERB
eurjchem-1700	35	40	towards	towards	ADP
eurjchem-1700	35	41	the	the	DET
eurjchem-1700	35	42	determination	determination	NOUN
eurjchem-1700	35	43	of	of	ADP
eurjchem-1700	35	44	clobetasone	clobetasone	NOUN
eurjchem-1700	35	45	butyrate	butyrate	NOUN
eurjchem-1700	35	46	both	both	CCONJ
eurjchem-1700	35	47	in	in	ADP
eurjchem-1700	35	48	bulk	bulk	NOUN
eurjchem-1700	35	49	as	as	ADV
eurjchem-1700	35	50	well	well	ADV
eurjchem-1700	35	51	as	as	ADP
eurjchem-1700	35	52	in	in	ADP
eurjchem-1700	35	53	topical	topical	ADJ
eurjchem-1700	35	54	formulations	formulation	NOUN
eurjchem-1700	35	55	.	.	PUNCT
eurjchem-1700	36	1	only	only	ADV
eurjchem-1700	36	2	one	one	NUM
eurjchem-1700	36	3	method	method	NOUN
eurjchem-1700	36	4	based	base	VERB
eurjchem-1700	36	5	on	on	ADP
eurjchem-1700	36	6	chromategraphic	chromategraphic	ADJ
eurjchem-1700	36	7	determination	determination	NOUN
eurjchem-1700	36	8	of	of	ADP
eurjchem-1700	36	9	clobetasone	clobetasone	NOUN
eurjchem-1700	36	10	butyrate	butyrate	NOUN
eurjchem-1700	36	11	in	in	ADP
eurjchem-1700	36	12	ointment	ointment	NOUN
eurjchem-1700	36	13	preparation	preparation	NOUN
eurjchem-1700	36	14	could	could	AUX
eurjchem-1700	36	15	be	be	AUX
eurjchem-1700	36	16	found	find	VERB
eurjchem-1700	36	17	[	[	X
eurjchem-1700	36	18	8	8	NUM
eurjchem-1700	36	19	]	]	PUNCT
eurjchem-1700	36	20	.	.	PUNCT
eurjchem-1700	37	1	on	on	ADP
eurjchem-1700	37	2	the	the	DET
eurjchem-1700	37	3	other	other	ADJ
eurjchem-1700	37	4	hand	hand	NOUN
eurjchem-1700	37	5	considerable	considerable	ADJ
eurjchem-1700	37	6	interest	interest	NOUN
eurjchem-1700	37	7	was	be	AUX
eurjchem-1700	37	8	shown	show	VERB
eurjchem-1700	37	9	to	to	ADP
eurjchem-1700	37	10	the	the	DET
eurjchem-1700	37	11	analysis	analysis	NOUN
eurjchem-1700	37	12	of	of	ADP
eurjchem-1700	37	13	propionate	propionate	ADJ
eurjchem-1700	37	14	ester	ester	NOUN
eurjchem-1700	37	15	of	of	ADP
eurjchem-1700	37	16	clobetasone	clobetasone	NOUN
eurjchem-1700	37	17	and	and	CCONJ
eurjchem-1700	37	18	hence	hence	ADV
eurjchem-1700	37	19	,	,	PUNCT
eurjchem-1700	37	20	several	several	ADJ
eurjchem-1700	37	21	analytical	analytical	ADJ
eurjchem-1700	37	22	methods	method	NOUN
eurjchem-1700	37	23	based	base	VERB
eurjchem-1700	37	24	on	on	ADP
eurjchem-1700	37	25	hplc	hplc	NOUN
eurjchem-1700	37	26	have	have	AUX
eurjchem-1700	37	27	been	be	AUX
eurjchem-1700	37	28	reported	report	VERB
eurjchem-1700	37	29	for	for	ADP
eurjchem-1700	37	30	its	its	PRON
eurjchem-1700	37	31	determination	determination	NOUN
eurjchem-1700	37	32	in	in	ADP
eurjchem-1700	37	33	pure	pure	ADJ
eurjchem-1700	37	34	and	and	CCONJ
eurjchem-1700	37	35	topical	topical	ADJ
eurjchem-1700	37	36	formulations	formulation	NOUN
eurjchem-1700	37	37	,	,	PUNCT
eurjchem-1700	37	38	either	either	CCONJ
eurjchem-1700	37	39	in	in	ADP
eurjchem-1700	37	40	single	single	ADJ
eurjchem-1700	37	41	or	or	CCONJ
eurjchem-1700	37	42	in	in	ADP
eurjchem-1700	37	43	combination	combination	NOUN
eurjchem-1700	37	44	with	with	ADP
eurjchem-1700	37	45	other	other	ADJ
eurjchem-1700	37	46	drugs	drug	NOUN
eurjchem-1700	37	47	[	[	X
eurjchem-1700	37	48	4,9	4,9	NUM
eurjchem-1700	37	49	-	-	SYM
eurjchem-1700	37	50	13	13	NUM
eurjchem-1700	37	51	]	]	PUNCT
eurjchem-1700	37	52	.	.	PUNCT
eurjchem-1700	38	1	to	to	ADP
eurjchem-1700	38	2	the	the	DET
eurjchem-1700	38	3	extent	extent	NOUN
eurjchem-1700	38	4	of	of	ADP
eurjchem-1700	38	5	our	our	PRON
eurjchem-1700	38	6	knowledge	knowledge	NOUN
eurjchem-1700	38	7	,	,	PUNCT
eurjchem-1700	38	8	no	no	DET
eurjchem-1700	38	9	hplc	hplc	NOUN
eurjchem-1700	38	10	method	method	NOUN
eurjchem-1700	38	11	for	for	ADP
eurjchem-1700	38	12	quantitative	quantitative	ADJ
eurjchem-1700	38	13	analysis	analysis	NOUN
eurjchem-1700	38	14	of	of	ADP
eurjchem-1700	38	15	clobetasone	clobetasone	NOUN
eurjchem-1700	38	16	butyrate	butyrate	NOUN
eurjchem-1700	38	17	in	in	ADP
eurjchem-1700	38	18	cream	cream	NOUN
eurjchem-1700	38	19	formulation	formulation	NOUN
eurjchem-1700	38	20	has	have	AUX
eurjchem-1700	38	21	been	be	AUX
eurjchem-1700	38	22	reported	report	VERB
eurjchem-1700	38	23	so	so	ADV
eurjchem-1700	38	24	far	far	ADV
eurjchem-1700	38	25	.	.	PUNCT
eurjchem-1700	39	1	as	as	ADP
eurjchem-1700	39	2	a	a	DET
eurjchem-1700	39	3	consequence	consequence	NOUN
eurjchem-1700	39	4	,	,	PUNCT
eurjchem-1700	39	5	in	in	ADP
eurjchem-1700	39	6	the	the	DET
eurjchem-1700	39	7	present	present	ADJ
eurjchem-1700	39	8	study	study	NOUN
eurjchem-1700	39	9	,	,	PUNCT
eurjchem-1700	39	10	a	a	DET
eurjchem-1700	39	11	stability	stability	NOUN
eurjchem-1700	39	12	indicating	indicate	VERB
eurjchem-1700	39	13	liquid	liquid	ADJ
eurjchem-1700	39	14	chromategraphic	chromategraphic	ADJ
eurjchem-1700	39	15	method	method	NOUN
eurjchem-1700	39	16	for	for	ADP
eurjchem-1700	39	17	determination	determination	NOUN
eurjchem-1700	39	18	of	of	ADP
eurjchem-1700	39	19	clobetasone	clobetasone	NOUN
eurjchem-1700	39	20	butyrate	butyrate	NOUN
eurjchem-1700	39	21	in	in	ADP
eurjchem-1700	39	22	bulk	bulk	ADJ
eurjchem-1700	39	23	and	and	CCONJ
eurjchem-1700	39	24	cream	cream	NOUN
eurjchem-1700	39	25	formulation	formulation	NOUN
eurjchem-1700	39	26	has	have	AUX
eurjchem-1700	39	27	been	be	AUX
eurjchem-1700	39	28	developed	develop	VERB
eurjchem-1700	39	29	and	and	CCONJ
eurjchem-1700	39	30	validated	validate	VERB
eurjchem-1700	39	31	in	in	ADP
eurjchem-1700	39	32	accordance	accordance	NOUN
eurjchem-1700	39	33	with	with	ADP
eurjchem-1700	39	34	international	international	ADJ
eurjchem-1700	39	35	conference	conference	NOUN
eurjchem-1700	39	36	on	on	ADP
eurjchem-1700	39	37	harmonization	harmonization	NOUN
eurjchem-1700	39	38	(	(	PUNCT
eurjchem-1700	39	39	ich	ich	NOUN
eurjchem-1700	39	40	)	)	PUNCT
eurjchem-1700	39	41	guidelines	guideline	VERB
eurjchem-1700	39	42	q2	q2	NOUN
eurjchem-1700	39	43	r1	r1	PROPN
eurjchem-1700	40	1	[	[	X
eurjchem-1700	40	2	14	14	NUM
eurjchem-1700	40	3	]	]	PUNCT
eurjchem-1700	40	4	.	.	PUNCT
eurjchem-1700	41	1	the	the	DET
eurjchem-1700	41	2	method	method	NOUN
eurjchem-1700	41	3	would	would	AUX
eurjchem-1700	41	4	be	be	AUX
eurjchem-1700	41	5	suitable	suitable	ADJ
eurjchem-1700	41	6	for	for	ADP
eurjchem-1700	41	7	routine	routine	ADJ
eurjchem-1700	41	8	quantification	quantification	NOUN
eurjchem-1700	41	9	of	of	ADP
eurjchem-1700	41	10	clobetasone	clobetasone	NOUN
eurjchem-1700	41	11	cream	cream	NOUN
eurjchem-1700	41	12	samples	sample	NOUN
eurjchem-1700	41	13	in	in	ADP
eurjchem-1700	41	14	pharmaceutical	pharmaceutical	ADJ
eurjchem-1700	41	15	quality	quality	NOUN
eurjchem-1700	41	16	control	control	NOUN
eurjchem-1700	41	17	laboratories	laboratory	NOUN
eurjchem-1700	41	18	.	.	PUNCT
eurjchem-1700	42	1	2	2	X
eurjchem-1700	42	2	.	.	X
eurjchem-1700	42	3	experimental	experimental	ADJ
eurjchem-1700	42	4	2.1	2.1	NUM
eurjchem-1700	42	5	.	.	PUNCT
eurjchem-1700	42	6	materials	material	NOUN
eurjchem-1700	42	7	the	the	DET
eurjchem-1700	42	8	clobetasone	clobetasone	NOUN
eurjchem-1700	42	9	butyrate	butyrate	NOUN
eurjchem-1700	42	10	reference	reference	NOUN
eurjchem-1700	42	11	standard	standard	NOUN
eurjchem-1700	42	12	(	(	PUNCT
eurjchem-1700	42	13	rs	rs	NOUN
eurjchem-1700	42	14	)	)	PUNCT
eurjchem-1700	42	15	was	be	AUX
eurjchem-1700	42	16	purchased	purchase	VERB
eurjchem-1700	42	17	from	from	ADP
eurjchem-1700	42	18	sigma	sigma	PROPN
eurjchem-1700	42	19	aldrich	aldrich	PROPN
eurjchem-1700	42	20	,	,	PUNCT
eurjchem-1700	42	21	(	(	PUNCT
eurjchem-1700	42	22	steinheim	steinheim	PROPN
eurjchem-1700	42	23	,	,	PUNCT
eurjchem-1700	42	24	germany	germany	PROPN
eurjchem-1700	42	25	)	)	PUNCT
eurjchem-1700	42	26	.	.	PUNCT
eurjchem-1700	43	1	the	the	DET
eurjchem-1700	43	2	eumovate	eumovate	NOUN
eurjchem-1700	43	3	(	(	PUNCT
eurjchem-1700	43	4	clobetasone	clobetasone	NOUN
eurjchem-1700	43	5	butyrate	butyrate	NOUN
eurjchem-1700	43	6	0.05	0.05	NUM
eurjchem-1700	43	7	%	%	NOUN
eurjchem-1700	43	8	)	)	PUNCT
eurjchem-1700	43	9	cream	cream	NOUN
eurjchem-1700	43	10	marketed	market	VERB
eurjchem-1700	43	11	by	by	ADP
eurjchem-1700	43	12	glaxo	glaxo	NOUN
eurjchem-1700	43	13	-	-	PUNCT
eurjchem-1700	43	14	smithkline	smithkline	PROPN
eurjchem-1700	43	15	,	,	PUNCT
eurjchem-1700	43	16	usa	usa	PROPN
eurjchem-1700	43	17	was	be	AUX
eurjchem-1700	43	18	procured	procure	VERB
eurjchem-1700	43	19	from	from	ADP
eurjchem-1700	43	20	local	local	ADJ
eurjchem-1700	43	21	pharmacy	pharmacy	NOUN
eurjchem-1700	43	22	shop	shop	NOUN
eurjchem-1700	43	23	(	(	PUNCT
eurjchem-1700	43	24	jazan	jazan	NOUN
eurjchem-1700	43	25	,	,	PUNCT
eurjchem-1700	43	26	kingdom	kingdom	NOUN
eurjchem-1700	43	27	of	of	ADP
eurjchem-1700	43	28	saudi	saudi	PROPN
eurjchem-1700	43	29	arabia	arabia	PROPN
eurjchem-1700	43	30	)	)	PUNCT
eurjchem-1700	43	31	.	.	PUNCT
eurjchem-1700	44	1	the	the	DET
eurjchem-1700	44	2	hplc	hplc	NOUN
eurjchem-1700	44	3	grade	grade	NOUN
eurjchem-1700	44	4	methanol	methanol	NOUN
eurjchem-1700	44	5	was	be	AUX
eurjchem-1700	44	6	purchased	purchase	VERB
eurjchem-1700	44	7	from	from	ADP
eurjchem-1700	44	8	merck	merck	PROPN
eurjchem-1700	44	9	,	,	PUNCT
eurjchem-1700	44	10	germany	germany	PROPN
eurjchem-1700	44	11	.	.	PUNCT
eurjchem-1700	45	1	hydrochloric	hydrochloric	ADJ
eurjchem-1700	45	2	acid	acid	NOUN
eurjchem-1700	45	3	,	,	PUNCT
eurjchem-1700	45	4	orthophosphoric	orthophosphoric	ADJ
eurjchem-1700	45	5	acid	acid	NOUN
eurjchem-1700	45	6	,	,	PUNCT
eurjchem-1700	45	7	30	30	NUM
eurjchem-1700	45	8	%	%	NOUN
eurjchem-1700	45	9	hydrogen	hydrogen	NOUN
eurjchem-1700	45	10	peroxide	peroxide	NOUN
eurjchem-1700	45	11	and	and	CCONJ
eurjchem-1700	45	12	sodium	sodium	NOUN
eurjchem-1700	45	13	hydroxide	hydroxide	NOUN
eurjchem-1700	45	14	were	be	AUX
eurjchem-1700	45	15	purchased	purchase	VERB
eurjchem-1700	45	16	from	from	ADP
eurjchem-1700	45	17	sigma	sigma	PROPN
eurjchem-1700	45	18	aldrich	aldrich	PROPN
eurjchem-1700	45	19	(	(	PUNCT
eurjchem-1700	45	20	steinheim	steinheim	PROPN
eurjchem-1700	45	21	,	,	PUNCT
eurjchem-1700	45	22	germany	germany	PROPN
eurjchem-1700	45	23	)	)	PUNCT
eurjchem-1700	45	24	.	.	PUNCT
eurjchem-1700	46	1	the	the	DET
eurjchem-1700	46	2	hplc	hplc	NOUN
eurjchem-1700	46	3	grade	grade	NOUN
eurjchem-1700	46	4	water	water	NOUN
eurjchem-1700	46	5	used	use	VERB
eurjchem-1700	46	6	throughout	throughout	ADP
eurjchem-1700	46	7	the	the	DET
eurjchem-1700	46	8	analysis	analysis	NOUN
eurjchem-1700	46	9	was	be	AUX
eurjchem-1700	46	10	produced	produce	VERB
eurjchem-1700	46	11	in	in	ADP
eurjchem-1700	46	12	our	our	PRON
eurjchem-1700	46	13	laboratory	laboratory	NOUN
eurjchem-1700	46	14	using	use	VERB
eurjchem-1700	46	15	milli	milli	ADJ
eurjchem-1700	46	16	-	-	PUNCT
eurjchem-1700	46	17	q	q	NOUN
eurjchem-1700	46	18	water	water	NOUN
eurjchem-1700	46	19	purification	purification	NOUN
eurjchem-1700	46	20	system	system	NOUN
eurjchem-1700	46	21	(	(	PUNCT
eurjchem-1700	46	22	millipore	millipore	PROPN
eurjchem-1700	46	23	,	,	PUNCT
eurjchem-1700	46	24	molsheim	molsheim	PROPN
eurjchem-1700	46	25	,	,	PUNCT
eurjchem-1700	46	26	france	france	PROPN
eurjchem-1700	46	27	)	)	PUNCT
eurjchem-1700	46	28	.	.	PUNCT
eurjchem-1700	47	1	all	all	DET
eurjchem-1700	47	2	the	the	DET
eurjchem-1700	47	3	analytical	analytical	ADJ
eurjchem-1700	47	4	solutions	solution	NOUN
eurjchem-1700	47	5	have	have	AUX
eurjchem-1700	47	6	been	be	AUX
eurjchem-1700	47	7	filtered	filter	VERB
eurjchem-1700	47	8	through	through	ADP
eurjchem-1700	47	9	0.22	0.22	NUM
eurjchem-1700	47	10	μ	μ	NOUN
eurjchem-1700	47	11	nylon	nylon	NOUN
eurjchem-1700	47	12	syringe	syringe	NOUN
eurjchem-1700	47	13	filter	filter	NOUN
eurjchem-1700	47	14	(	(	PUNCT
eurjchem-1700	47	15	millipore	millipore	PROPN
eurjchem-1700	47	16	,	,	PUNCT
eurjchem-1700	47	17	molsheim	molsheim	PROPN
eurjchem-1700	47	18	,	,	PUNCT
eurjchem-1700	47	19	france	france	PROPN
eurjchem-1700	47	20	)	)	PUNCT
eurjchem-1700	47	21	before	before	ADP
eurjchem-1700	47	22	injection	injection	NOUN
eurjchem-1700	47	23	into	into	ADP
eurjchem-1700	47	24	hplc	hplc	NOUN
eurjchem-1700	47	25	system	system	NOUN
eurjchem-1700	47	26	.	.	PUNCT
eurjchem-1700	48	1	2.2	2.2	NUM
eurjchem-1700	48	2	.	.	PUNCT
eurjchem-1700	48	3	equipments	equipment	NOUN
eurjchem-1700	48	4	and	and	CCONJ
eurjchem-1700	48	5	chromatographic	chromatographic	ADJ
eurjchem-1700	48	6	conditions	condition	NOUN
eurjchem-1700	48	7	all	all	DET
eurjchem-1700	48	8	the	the	DET
eurjchem-1700	48	9	chromatographic	chromatographic	ADJ
eurjchem-1700	48	10	analysis	analysis	NOUN
eurjchem-1700	48	11	was	be	AUX
eurjchem-1700	48	12	carried	carry	VERB
eurjchem-1700	48	13	out	out	ADP
eurjchem-1700	48	14	on	on	ADP
eurjchem-1700	48	15	shimadzu	shimadzu	ADJ
eurjchem-1700	48	16	lc-20	lc-20	NOUN
eurjchem-1700	48	17	at	at	ADP
eurjchem-1700	48	18	hplc	hplc	NOUN
eurjchem-1700	48	19	system	system	NOUN
eurjchem-1700	48	20	(	(	PUNCT
eurjchem-1700	48	21	tokyo	tokyo	PROPN
eurjchem-1700	48	22	,	,	PUNCT
eurjchem-1700	48	23	japan	japan	PROPN
eurjchem-1700	48	24	)	)	PUNCT
eurjchem-1700	48	25	equipped	equip	VERB
eurjchem-1700	48	26	with	with	ADP
eurjchem-1700	48	27	photodiode	photodiode	NOUN
eurjchem-1700	48	28	array	array	NOUN
eurjchem-1700	48	29	(	(	PUNCT
eurjchem-1700	48	30	pda	pda	NOUN
eurjchem-1700	48	31	)	)	PUNCT
eurjchem-1700	48	32	detector	detector	NOUN
eurjchem-1700	48	33	covering	cover	VERB
eurjchem-1700	48	34	a	a	DET
eurjchem-1700	48	35	range	range	NOUN
eurjchem-1700	48	36	of	of	ADP
eurjchem-1700	48	37	190400	190400	NUM
eurjchem-1700	48	38	nm	nm	NOUN
eurjchem-1700	48	39	(	(	PUNCT
eurjchem-1700	48	40	spd	spd	NOUN
eurjchem-1700	48	41	-	-	PUNCT
eurjchem-1700	48	42	m20a	m20a	NOUN
eurjchem-1700	48	43	)	)	PUNCT
eurjchem-1700	48	44	,	,	PUNCT
eurjchem-1700	48	45	autosampler	autosampler	NOUN
eurjchem-1700	48	46	(	(	PUNCT
eurjchem-1700	48	47	sil-20a	sil-20a	NOUN
eurjchem-1700	48	48	)	)	PUNCT
eurjchem-1700	48	49	and	and	CCONJ
eurjchem-1700	48	50	column	column	NOUN
eurjchem-1700	48	51	thermostat	thermostat	PROPN
eurjchem-1700	48	52	chamber	chamber	PROPN
eurjchem-1700	48	53	(	(	PUNCT
eurjchem-1700	48	54	cto-20a	cto-20a	NUM
eurjchem-1700	48	55	)	)	PUNCT
eurjchem-1700	48	56	.	.	PUNCT
eurjchem-1700	49	1	analytical	analytical	ADJ
eurjchem-1700	49	2	balance	balance	NOUN
eurjchem-1700	49	3	(	(	PUNCT
eurjchem-1700	49	4	metler	metler	PROPN
eurjchem-1700	49	5	toledo	toledo	PROPN
eurjchem-1700	49	6	,	,	PUNCT
eurjchem-1700	49	7	usa	usa	PROPN
eurjchem-1700	49	8	)	)	PUNCT
eurjchem-1700	49	9	,	,	PUNCT
eurjchem-1700	49	10	hot	hot	ADJ
eurjchem-1700	49	11	air	air	NOUN
eurjchem-1700	49	12	oven	oven	NOUN
eurjchem-1700	49	13	(	(	PUNCT
eurjchem-1700	49	14	sel	sel	NOUN
eurjchem-1700	49	15	lab	lab	NOUN
eurjchem-1700	49	16	,	,	PUNCT
eurjchem-1700	49	17	sheldon	sheldon	PROPN
eurjchem-1700	49	18	manufacturing	manufacturing	PROPN
eurjchem-1700	49	19	inc	inc	PROPN
eurjchem-1700	49	20	.	.	PROPN
eurjchem-1700	49	21	usa	usa	PROPN
eurjchem-1700	49	22	)	)	PUNCT
eurjchem-1700	49	23	,	,	PUNCT
eurjchem-1700	49	24	digital	digital	ADJ
eurjchem-1700	49	25	water	water	NOUN
eurjchem-1700	49	26	bath	bath	NOUN
eurjchem-1700	49	27	(	(	PUNCT
eurjchem-1700	49	28	daihan	daihan	PROPN
eurjchem-1700	49	29	labtech	labtech	PROPN
eurjchem-1700	49	30	,	,	PUNCT
eurjchem-1700	49	31	korea	korea	PROPN
eurjchem-1700	49	32	)	)	PUNCT
eurjchem-1700	49	33	and	and	CCONJ
eurjchem-1700	49	34	ultrasonicator	ultrasonicator	NOUN
eurjchem-1700	49	35	(	(	PUNCT
eurjchem-1700	49	36	wisd	wisd	ADV
eurjchem-1700	49	37	,	,	PUNCT
eurjchem-1700	49	38	dathan	dathan	ADV
eurjchem-1700	49	39	scientific	scientific	ADJ
eurjchem-1700	49	40	,	,	PUNCT
eurjchem-1700	49	41	korea	korea	PROPN
eurjchem-1700	49	42	)	)	PUNCT
eurjchem-1700	49	43	were	be	AUX
eurjchem-1700	49	44	used	use	VERB
eurjchem-1700	49	45	during	during	ADP
eurjchem-1700	49	46	the	the	DET
eurjchem-1700	49	47	experiment	experiment	NOUN
eurjchem-1700	49	48	.	.	PUNCT
eurjchem-1700	50	1	the	the	DET
eurjchem-1700	50	2	chromatographic	chromatographic	ADJ
eurjchem-1700	50	3	analysis	analysis	NOUN
eurjchem-1700	50	4	was	be	AUX
eurjchem-1700	50	5	carried	carry	VERB
eurjchem-1700	50	6	out	out	ADP
eurjchem-1700	50	7	on	on	ADP
eurjchem-1700	50	8	isocratic	isocratic	ADJ
eurjchem-1700	50	9	mode	mode	NOUN
eurjchem-1700	50	10	and	and	CCONJ
eurjchem-1700	50	11	separation	separation	NOUN
eurjchem-1700	50	12	was	be	AUX
eurjchem-1700	50	13	obtained	obtain	VERB
eurjchem-1700	50	14	by	by	ADP
eurjchem-1700	50	15	using	use	VERB
eurjchem-1700	50	16	zodiac	zodiac	PROPN
eurjchem-1700	50	17	c18	c18	NOUN
eurjchem-1700	50	18	column	column	NOUN
eurjchem-1700	50	19	(	(	PUNCT
eurjchem-1700	50	20	50	50	NUM
eurjchem-1700	50	21	mm	mm	NOUN
eurjchem-1700	50	22	×	×	NOUN
eurjchem-1700	50	23	4.6	4.6	NUM
eurjchem-1700	50	24	mm	mm	NOUN
eurjchem-1700	50	25	,	,	PUNCT
eurjchem-1700	50	26	5	5	NUM
eurjchem-1700	50	27	μm	μm	NOUN
eurjchem-1700	50	28	)	)	PUNCT
eurjchem-1700	50	29	as	as	ADP
eurjchem-1700	50	30	stationary	stationary	ADJ
eurjchem-1700	50	31	phase	phase	NOUN
eurjchem-1700	50	32	and	and	CCONJ
eurjchem-1700	50	33	a	a	DET
eurjchem-1700	50	34	mixture	mixture	NOUN
eurjchem-1700	50	35	of	of	ADP
eurjchem-1700	50	36	water	water	NOUN
eurjchem-1700	50	37	and	and	CCONJ
eurjchem-1700	50	38	methanol	methanol	NOUN
eurjchem-1700	50	39	(	(	PUNCT
eurjchem-1700	50	40	16:84	16:84	NUM
eurjchem-1700	50	41	,	,	PUNCT
eurjchem-1700	50	42	v	v	ADP
eurjchem-1700	50	43	:	:	SYM
eurjchem-1700	50	44	v	v	NOUN
eurjchem-1700	50	45	,	,	PUNCT
eurjchem-1700	50	46	ph	ph	PROPN
eurjchem-1700	50	47	adjusted	adjust	VERB
eurjchem-1700	50	48	to	to	ADP
eurjchem-1700	50	49	6.0	6.0	NUM
eurjchem-1700	50	50	with	with	ADP
eurjchem-1700	50	51	o	o	ADJ
eurjchem-1700	50	52	-	-	ADJ
eurjchem-1700	50	53	phosphoric	phosphoric	ADJ
eurjchem-1700	50	54	acid	acid	NOUN
eurjchem-1700	50	55	)	)	PUNCT
eurjchem-1700	50	56	was	be	AUX
eurjchem-1700	50	57	used	use	VERB
eurjchem-1700	50	58	as	as	ADP
eurjchem-1700	50	59	mobile	mobile	ADJ
eurjchem-1700	50	60	phase	phase	NOUN
eurjchem-1700	50	61	.	.	PUNCT
eurjchem-1700	51	1	a	a	DET
eurjchem-1700	51	2	column	column	NOUN
eurjchem-1700	51	3	temperature	temperature	NOUN
eurjchem-1700	51	4	of	of	ADP
eurjchem-1700	51	5	27	27	NUM
eurjchem-1700	51	6	°	°	NOUN
eurjchem-1700	51	7	c	c	NOUN
eurjchem-1700	51	8	was	be	AUX
eurjchem-1700	51	9	maintained	maintain	VERB
eurjchem-1700	51	10	,	,	PUNCT
eurjchem-1700	51	11	1	1	NUM
eurjchem-1700	51	12	ml	ml	NOUN
eurjchem-1700	51	13	/	/	SYM
eurjchem-1700	51	14	min	min	NOUN
eurjchem-1700	51	15	effluent	effluent	ADJ
eurjchem-1700	51	16	flow	flow	NOUN
eurjchem-1700	51	17	rate	rate	NOUN
eurjchem-1700	51	18	,	,	PUNCT
eurjchem-1700	51	19	20	20	NUM
eurjchem-1700	51	20	μl	μl	ADP
eurjchem-1700	51	21	injection	injection	NOUN
eurjchem-1700	51	22	volume	volume	NOUN
eurjchem-1700	51	23	and	and	CCONJ
eurjchem-1700	51	24	15	15	NUM
eurjchem-1700	51	25	min	min	NOUN
eurjchem-1700	51	26	runtime	runtime	NOUN
eurjchem-1700	51	27	were	be	AUX
eurjchem-1700	51	28	set	set	VERB
eurjchem-1700	51	29	throughout	throughout	ADP
eurjchem-1700	51	30	the	the	DET
eurjchem-1700	51	31	analysis	analysis	NOUN
eurjchem-1700	51	32	.	.	PUNCT
eurjchem-1700	52	1	the	the	DET
eurjchem-1700	52	2	data	datum	NOUN
eurjchem-1700	52	3	were	be	AUX
eurjchem-1700	52	4	acquired	acquire	VERB
eurjchem-1700	52	5	at	at	ADP
eurjchem-1700	52	6	a	a	DET
eurjchem-1700	52	7	detection	detection	NOUN
eurjchem-1700	52	8	wavelength	wavelength	NOUN
eurjchem-1700	52	9	of	of	ADP
eurjchem-1700	52	10	240	240	NUM
eurjchem-1700	52	11	nm	nm	NOUN
eurjchem-1700	52	12	.	.	PUNCT
eurjchem-1700	53	1	the	the	DET
eurjchem-1700	53	2	hplc	hplc	NOUN
eurjchem-1700	53	3	system	system	NOUN
eurjchem-1700	53	4	was	be	AUX
eurjchem-1700	53	5	monitored	monitor	VERB
eurjchem-1700	53	6	and	and	CCONJ
eurjchem-1700	53	7	the	the	DET
eurjchem-1700	53	8	data	datum	NOUN
eurjchem-1700	53	9	were	be	AUX
eurjchem-1700	53	10	processed	process	VERB
eurjchem-1700	53	11	using	use	VERB
eurjchem-1700	53	12	shimadzu	shimadzu	ADJ
eurjchem-1700	53	13	lc	lc	NOUN
eurjchem-1700	53	14	-	-	PUNCT
eurjchem-1700	53	15	solution	solution	NOUN
eurjchem-1700	53	16	software	software	NOUN
eurjchem-1700	53	17	.	.	PUNCT
eurjchem-1700	54	1	the	the	DET
eurjchem-1700	54	2	mobile	mobile	ADJ
eurjchem-1700	54	3	phase	phase	NOUN
eurjchem-1700	54	4	was	be	AUX
eurjchem-1700	54	5	used	use	VERB
eurjchem-1700	54	6	as	as	ADP
eurjchem-1700	54	7	diluent	diluent	NOUN
eurjchem-1700	54	8	.	.	PUNCT
eurjchem-1700	55	1	2.3	2.3	NUM
eurjchem-1700	55	2	.	.	PUNCT
eurjchem-1700	56	1	preparation	preparation	NOUN
eurjchem-1700	56	2	of	of	ADP
eurjchem-1700	56	3	standard	standard	ADJ
eurjchem-1700	56	4	solution	solution	NOUN
eurjchem-1700	56	5	the	the	DET
eurjchem-1700	56	6	stock	stock	NOUN
eurjchem-1700	56	7	standard	standard	ADJ
eurjchem-1700	56	8	solution	solution	NOUN
eurjchem-1700	56	9	was	be	AUX
eurjchem-1700	56	10	prepared	prepare	VERB
eurjchem-1700	56	11	by	by	ADP
eurjchem-1700	56	12	transferring	transfer	VERB
eurjchem-1700	56	13	an	an	DET
eurjchem-1700	56	14	appropriate	appropriate	ADJ
eurjchem-1700	56	15	quantity	quantity	NOUN
eurjchem-1700	56	16	of	of	ADP
eurjchem-1700	56	17	clobetasone	clobetasone	NOUN
eurjchem-1700	56	18	butyrate	butyrate	NOUN
eurjchem-1700	56	19	reference	reference	NOUN
eurjchem-1700	56	20	standard	standard	NOUN
eurjchem-1700	56	21	in	in	ADP
eurjchem-1700	56	22	a	a	DET
eurjchem-1700	56	23	volumetric	volumetric	NOUN
eurjchem-1700	56	24	flask	flask	NOUN
eurjchem-1700	56	25	,	,	PUNCT
eurjchem-1700	56	26	dissolved	dissolve	VERB
eurjchem-1700	56	27	in	in	ADP
eurjchem-1700	56	28	mobile	mobile	ADJ
eurjchem-1700	56	29	phase	phase	NOUN
eurjchem-1700	56	30	by	by	ADP
eurjchem-1700	56	31	sonicating	sonicate	VERB
eurjchem-1700	56	32	for	for	ADP
eurjchem-1700	56	33	5	5	NUM
eurjchem-1700	56	34	min	min	NOUN
eurjchem-1700	56	35	and	and	CCONJ
eurjchem-1700	56	36	volume	volume	NOUN
eurjchem-1700	56	37	was	be	AUX
eurjchem-1700	56	38	made	make	VERB
eurjchem-1700	56	39	up	up	ADP
eurjchem-1700	56	40	with	with	ADP
eurjchem-1700	56	41	mobile	mobile	ADJ
eurjchem-1700	56	42	phase	phase	NOUN
eurjchem-1700	56	43	to	to	PART
eurjchem-1700	56	44	achieve	achieve	VERB
eurjchem-1700	56	45	a	a	DET
eurjchem-1700	56	46	solution	solution	NOUN
eurjchem-1700	56	47	of	of	ADP
eurjchem-1700	56	48	1	1	NUM
eurjchem-1700	56	49	mg	mg	NUM
eurjchem-1700	56	50	/	/	SYM
eurjchem-1700	56	51	ml	ml	NOUN
eurjchem-1700	56	52	concentration	concentration	NOUN
eurjchem-1700	56	53	.	.	PUNCT
eurjchem-1700	57	1	the	the	DET
eurjchem-1700	57	2	working	work	VERB
eurjchem-1700	57	3	standard	standard	ADJ
eurjchem-1700	57	4	solution	solution	NOUN
eurjchem-1700	57	5	(	(	PUNCT
eurjchem-1700	57	6	25	25	NUM
eurjchem-1700	57	7	μg	μg	NOUN
eurjchem-1700	57	8	/	/	SYM
eurjchem-1700	57	9	ml	ml	NOUN
eurjchem-1700	57	10	)	)	PUNCT
eurjchem-1700	57	11	for	for	ADP
eurjchem-1700	57	12	method	method	NOUN
eurjchem-1700	57	13	development	development	NOUN
eurjchem-1700	57	14	was	be	AUX
eurjchem-1700	57	15	prepared	prepare	VERB
eurjchem-1700	57	16	from	from	ADP
eurjchem-1700	57	17	stock	stock	NOUN
eurjchem-1700	57	18	standard	standard	ADJ
eurjchem-1700	57	19	solution	solution	NOUN
eurjchem-1700	57	20	using	use	VERB
eurjchem-1700	57	21	mobile	mobile	ADJ
eurjchem-1700	57	22	phase	phase	NOUN
eurjchem-1700	57	23	as	as	ADP
eurjchem-1700	57	24	diluent	diluent	NOUN
eurjchem-1700	57	25	.	.	PUNCT
eurjchem-1700	58	1	the	the	DET
eurjchem-1700	58	2	standard	standard	ADJ
eurjchem-1700	58	3	stock	stock	NOUN
eurjchem-1700	58	4	solution	solution	NOUN
eurjchem-1700	58	5	was	be	AUX
eurjchem-1700	58	6	also	also	ADV
eurjchem-1700	58	7	diluted	dilute	VERB
eurjchem-1700	58	8	with	with	ADP
eurjchem-1700	58	9	mobile	mobile	ADJ
eurjchem-1700	58	10	phase	phase	NOUN
eurjchem-1700	58	11	to	to	PART
eurjchem-1700	58	12	prepare	prepare	VERB
eurjchem-1700	58	13	a	a	DET
eurjchem-1700	58	14	series	series	NOUN
eurjchem-1700	58	15	of	of	ADP
eurjchem-1700	58	16	working	work	VERB
eurjchem-1700	58	17	solutions	solution	NOUN
eurjchem-1700	58	18	of	of	ADP
eurjchem-1700	58	19	5	5	NUM
eurjchem-1700	58	20	-	-	SYM
eurjchem-1700	58	21	50	50	NUM
eurjchem-1700	58	22	μg	μg	NOUN
eurjchem-1700	58	23	/	/	SYM
eurjchem-1700	58	24	ml	ml	NOUN
eurjchem-1700	58	25	concentrations	concentration	NOUN
eurjchem-1700	58	26	,	,	PUNCT
eurjchem-1700	58	27	which	which	PRON
eurjchem-1700	58	28	were	be	AUX
eurjchem-1700	58	29	used	use	VERB
eurjchem-1700	58	30	for	for	ADP
eurjchem-1700	58	31	linearity	linearity	NOUN
eurjchem-1700	58	32	experiment	experiment	NOUN
eurjchem-1700	58	33	.	.	PUNCT
eurjchem-1700	59	1	the	the	DET
eurjchem-1700	59	2	above	above	ADP
eurjchem-1700	59	3	working	working	NOUN
eurjchem-1700	59	4	standard	standard	ADJ
eurjchem-1700	59	5	and	and	CCONJ
eurjchem-1700	59	6	linearity	linearity	NOUN
eurjchem-1700	59	7	solutions	solution	NOUN
eurjchem-1700	59	8	were	be	AUX
eurjchem-1700	59	9	injected	inject	VERB
eurjchem-1700	59	10	in	in	ADP
eurjchem-1700	59	11	the	the	DET
eurjchem-1700	59	12	system	system	NOUN
eurjchem-1700	59	13	and	and	CCONJ
eurjchem-1700	59	14	analysed	analyse	VERB
eurjchem-1700	59	15	in	in	ADP
eurjchem-1700	59	16	six	six	NUM
eurjchem-1700	59	17	replicates	replicate	NOUN
eurjchem-1700	59	18	.	.	PUNCT
eurjchem-1700	60	1	2.4	2.4	NUM
eurjchem-1700	60	2	.	.	PUNCT
eurjchem-1700	60	3	preparation	preparation	NOUN
eurjchem-1700	60	4	of	of	ADP
eurjchem-1700	60	5	sample	sample	NOUN
eurjchem-1700	60	6	solution	solution	NOUN
eurjchem-1700	60	7	an	an	PRON
eurjchem-1700	60	8	accurately	accurately	ADV
eurjchem-1700	60	9	weighed	weigh	VERB
eurjchem-1700	60	10	500	500	NUM
eurjchem-1700	60	11	mg	mg	NOUN
eurjchem-1700	60	12	of	of	ADP
eurjchem-1700	60	13	cream	cream	NOUN
eurjchem-1700	60	14	sample	sample	NOUN
eurjchem-1700	60	15	(	(	PUNCT
eurjchem-1700	60	16	equivalent	equivalent	ADJ
eurjchem-1700	60	17	to	to	ADP
eurjchem-1700	60	18	10	10	NUM
eurjchem-1700	60	19	mg	mg	NOUN
eurjchem-1700	60	20	of	of	ADP
eurjchem-1700	60	21	clobetasone	clobetasone	NOUN
eurjchem-1700	60	22	butyrate	butyrate	NOUN
eurjchem-1700	60	23	)	)	PUNCT
eurjchem-1700	60	24	was	be	AUX
eurjchem-1700	60	25	taken	take	VERB
eurjchem-1700	60	26	into	into	ADP
eurjchem-1700	60	27	a	a	DET
eurjchem-1700	60	28	100	100	NUM
eurjchem-1700	60	29	ml	ml	NOUN
eurjchem-1700	60	30	volumetric	volumetric	ADJ
eurjchem-1700	60	31	flask	flask	NOUN
eurjchem-1700	60	32	.	.	PUNCT
eurjchem-1700	61	1	approximately	approximately	ADV
eurjchem-1700	61	2	,	,	PUNCT
eurjchem-1700	61	3	60	60	NUM
eurjchem-1700	61	4	ml	ml	NOUN
eurjchem-1700	61	5	of	of	ADP
eurjchem-1700	61	6	diluent	diluent	NOUN
eurjchem-1700	61	7	was	be	AUX
eurjchem-1700	61	8	added	add	VERB
eurjchem-1700	61	9	to	to	ADP
eurjchem-1700	61	10	the	the	DET
eurjchem-1700	61	11	flask	flask	NOUN
eurjchem-1700	61	12	and	and	CCONJ
eurjchem-1700	61	13	sonicated	sonicate	VERB
eurjchem-1700	61	14	for	for	ADP
eurjchem-1700	61	15	20	20	NUM
eurjchem-1700	61	16	min	min	NOUN
eurjchem-1700	61	17	with	with	ADP
eurjchem-1700	61	18	occasional	occasional	ADJ
eurjchem-1700	61	19	shaking	shaking	NOUN
eurjchem-1700	61	20	and	and	CCONJ
eurjchem-1700	61	21	then	then	ADV
eurjchem-1700	61	22	the	the	DET
eurjchem-1700	61	23	final	final	ADJ
eurjchem-1700	61	24	volume	volume	NOUN
eurjchem-1700	61	25	was	be	AUX
eurjchem-1700	61	26	adjusted	adjust	VERB
eurjchem-1700	61	27	using	use	VERB
eurjchem-1700	61	28	mobile	mobile	ADJ
eurjchem-1700	61	29	phase	phase	NOUN
eurjchem-1700	61	30	as	as	ADP
eurjchem-1700	61	31	diluent	diluent	NOUN
eurjchem-1700	61	32	and	and	CCONJ
eurjchem-1700	61	33	mixed	mixed	ADJ
eurjchem-1700	61	34	thoroughly	thoroughly	ADV
eurjchem-1700	61	35	.	.	PUNCT
eurjchem-1700	62	1	further	further	ADJ
eurjchem-1700	62	2	dilutions	dilution	NOUN
eurjchem-1700	62	3	were	be	AUX
eurjchem-1700	62	4	made	make	VERB
eurjchem-1700	62	5	to	to	PART
eurjchem-1700	62	6	achieve	achieve	VERB
eurjchem-1700	62	7	required	required	ADJ
eurjchem-1700	62	8	concentrations	concentration	NOUN
eurjchem-1700	62	9	.	.	PUNCT
eurjchem-1700	63	1	prior	prior	ADV
eurjchem-1700	63	2	to	to	ADP
eurjchem-1700	63	3	injection	injection	NOUN
eurjchem-1700	63	4	,	,	PUNCT
eurjchem-1700	63	5	the	the	DET
eurjchem-1700	63	6	solution	solution	NOUN
eurjchem-1700	63	7	were	be	AUX
eurjchem-1700	63	8	filtered	filter	VERB
eurjchem-1700	63	9	using	use	VERB
eurjchem-1700	63	10	0.45	0.45	NUM
eurjchem-1700	63	11	μ	μ	PROPN
eurjchem-1700	63	12	nylon	nylon	NOUN
eurjchem-1700	63	13	filter	filter	NOUN
eurjchem-1700	63	14	.	.	PUNCT
eurjchem-1700	64	1	2.5	2.5	NUM
eurjchem-1700	64	2	.	.	PUNCT
eurjchem-1700	65	1	method	method	NOUN
eurjchem-1700	65	2	validation	validation	NOUN
eurjchem-1700	65	3	the	the	DET
eurjchem-1700	65	4	validation	validation	NOUN
eurjchem-1700	65	5	of	of	ADP
eurjchem-1700	65	6	the	the	DET
eurjchem-1700	65	7	proposed	propose	VERB
eurjchem-1700	65	8	method	method	NOUN
eurjchem-1700	65	9	was	be	AUX
eurjchem-1700	65	10	performed	perform	VERB
eurjchem-1700	65	11	in	in	ADP
eurjchem-1700	65	12	accordance	accordance	NOUN
eurjchem-1700	65	13	with	with	ADP
eurjchem-1700	65	14	the	the	DET
eurjchem-1700	65	15	ich	ich	PROPN
eurjchem-1700	65	16	guidelines	guideline	NOUN
eurjchem-1700	65	17	q2	q2	NOUN
eurjchem-1700	65	18	r1	r1	PROPN
eurjchem-1700	66	1	[	[	X
eurjchem-1700	66	2	14	14	NUM
eurjchem-1700	66	3	]	]	PUNCT
eurjchem-1700	66	4	.	.	PUNCT
eurjchem-1700	67	1	the	the	DET
eurjchem-1700	67	2	parameters	parameter	NOUN
eurjchem-1700	67	3	such	such	ADJ
eurjchem-1700	67	4	as	as	ADP
eurjchem-1700	67	5	system	system	NOUN
eurjchem-1700	67	6	suitability	suitability	NOUN
eurjchem-1700	67	7	,	,	PUNCT
eurjchem-1700	67	8	linearity	linearity	NOUN
eurjchem-1700	67	9	,	,	PUNCT
eurjchem-1700	67	10	limit	limit	NOUN
eurjchem-1700	67	11	of	of	ADP
eurjchem-1700	67	12	detection	detection	NOUN
eurjchem-1700	67	13	and	and	CCONJ
eurjchem-1700	67	14	limit	limit	NOUN
eurjchem-1700	67	15	of	of	ADP
eurjchem-1700	67	16	quantitation	quantitation	NOUN
eurjchem-1700	67	17	,	,	PUNCT
eurjchem-1700	67	18	precision	precision	NOUN
eurjchem-1700	67	19	,	,	PUNCT
eurjchem-1700	67	20	accuracy	accuracy	NOUN
eurjchem-1700	67	21	,	,	PUNCT
eurjchem-1700	67	22	specificity	specificity	NOUN
eurjchem-1700	67	23	-	-	PUNCT
eurjchem-1700	67	24	forced	force	VERB
eurjchem-1700	67	25	degradation	degradation	NOUN
eurjchem-1700	67	26	of	of	ADP
eurjchem-1700	67	27	cream	cream	NOUN
eurjchem-1700	67	28	samples	sample	NOUN
eurjchem-1700	67	29	and	and	CCONJ
eurjchem-1700	67	30	solution	solution	NOUN
eurjchem-1700	67	31	stability	stability	NOUN
eurjchem-1700	67	32	were	be	AUX
eurjchem-1700	67	33	assessed	assess	VERB
eurjchem-1700	67	34	.	.	PUNCT
eurjchem-1700	68	1	2.5.1	2.5.1	X
eurjchem-1700	68	2	.	.	PUNCT
eurjchem-1700	68	3	system	system	NOUN
eurjchem-1700	68	4	suitability	suitability	NOUN
eurjchem-1700	68	5	to	to	PART
eurjchem-1700	68	6	make	make	VERB
eurjchem-1700	68	7	sure	sure	ADJ
eurjchem-1700	68	8	that	that	SCONJ
eurjchem-1700	68	9	the	the	DET
eurjchem-1700	68	10	hplc	hplc	NOUN
eurjchem-1700	68	11	system	system	NOUN
eurjchem-1700	68	12	is	be	AUX
eurjchem-1700	68	13	appropriate	appropriate	ADJ
eurjchem-1700	68	14	for	for	ADP
eurjchem-1700	68	15	proposed	propose	VERB
eurjchem-1700	68	16	experiment	experiment	NOUN
eurjchem-1700	68	17	,	,	PUNCT
eurjchem-1700	68	18	the	the	DET
eurjchem-1700	68	19	system	system	NOUN
eurjchem-1700	68	20	suitability	suitability	NOUN
eurjchem-1700	68	21	parameters	parameter	NOUN
eurjchem-1700	68	22	such	such	ADJ
eurjchem-1700	68	23	as	as	ADP
eurjchem-1700	68	24	retention	retention	NOUN
eurjchem-1700	68	25	time	time	NOUN
eurjchem-1700	68	26	,	,	PUNCT
eurjchem-1700	68	27	number	number	NOUN
eurjchem-1700	68	28	of	of	ADP
eurjchem-1700	68	29	theoretical	theoretical	ADJ
eurjchem-1700	68	30	plates	plate	NOUN
eurjchem-1700	68	31	,	,	PUNCT
eurjchem-1700	68	32	tailing	tail	VERB
eurjchem-1700	68	33	factor	factor	NOUN
eurjchem-1700	68	34	of	of	ADP
eurjchem-1700	68	35	analyte	analyte	NOUN
eurjchem-1700	68	36	peak	peak	NOUN
eurjchem-1700	68	37	and	and	CCONJ
eurjchem-1700	68	38	percent	percent	NOUN
eurjchem-1700	68	39	rsd	rsd	NOUN
eurjchem-1700	68	40	of	of	ADP
eurjchem-1700	68	41	area	area	NOUN
eurjchem-1700	68	42	for	for	ADP
eurjchem-1700	68	43	six	six	NUM
eurjchem-1700	68	44	replicate	replicate	ADJ
eurjchem-1700	68	45	injections	injection	NOUN
eurjchem-1700	68	46	of	of	ADP
eurjchem-1700	68	47	analyte	analyte	NOUN
eurjchem-1700	68	48	were	be	AUX
eurjchem-1700	68	49	observed	observe	VERB
eurjchem-1700	68	50	at	at	ADP
eurjchem-1700	68	51	the	the	DET
eurjchem-1700	68	52	beginning	beginning	NOUN
eurjchem-1700	68	53	of	of	ADP
eurjchem-1700	68	54	the	the	DET
eurjchem-1700	68	55	experiment	experiment	NOUN
eurjchem-1700	68	56	and	and	CCONJ
eurjchem-1700	68	57	monitored	monitor	VERB
eurjchem-1700	68	58	throughout	throughout	ADP
eurjchem-1700	68	59	the	the	DET
eurjchem-1700	68	60	analysis	analysis	NOUN
eurjchem-1700	68	61	.	.	PUNCT
eurjchem-1700	69	1	for	for	ADP
eurjchem-1700	69	2	this	this	DET
eurjchem-1700	69	3	purpose	purpose	NOUN
eurjchem-1700	69	4	,	,	PUNCT
eurjchem-1700	69	5	working	working	NOUN
eurjchem-1700	69	6	standard	standard	ADJ
eurjchem-1700	69	7	solution	solution	NOUN
eurjchem-1700	69	8	(	(	PUNCT
eurjchem-1700	69	9	25	25	NUM
eurjchem-1700	69	10	μg	μg	NOUN
eurjchem-1700	69	11	/	/	SYM
eurjchem-1700	69	12	ml	ml	NOUN
eurjchem-1700	69	13	)	)	PUNCT
eurjchem-1700	69	14	was	be	AUX
eurjchem-1700	69	15	analysed	analyse	VERB
eurjchem-1700	69	16	and	and	CCONJ
eurjchem-1700	69	17	chromatograms	chromatogram	NOUN
eurjchem-1700	69	18	were	be	AUX
eurjchem-1700	69	19	recorded	record	VERB
eurjchem-1700	69	20	.	.	PUNCT
eurjchem-1700	70	1	the	the	DET
eurjchem-1700	70	2	number	number	NOUN
eurjchem-1700	70	3	of	of	ADP
eurjchem-1700	70	4	theoretical	theoretical	ADJ
eurjchem-1700	70	5	plate	plate	NOUN
eurjchem-1700	70	6	more	more	ADJ
eurjchem-1700	70	7	than	than	ADP
eurjchem-1700	70	8	3000	3000	NUM
eurjchem-1700	70	9	,	,	PUNCT
eurjchem-1700	70	10	tailing	tail	VERB
eurjchem-1700	70	11	factor	factor	NOUN
eurjchem-1700	70	12	(	(	PUNCT
eurjchem-1700	70	13	less	less	ADJ
eurjchem-1700	70	14	than	than	ADP
eurjchem-1700	70	15	1.5	1.5	NUM
eurjchem-1700	70	16	)	)	PUNCT
eurjchem-1700	70	17	and	and	CCONJ
eurjchem-1700	70	18	%	%	X
eurjchem-1700	70	19	rsd	rsd	NOUN
eurjchem-1700	70	20	of	of	ADP
eurjchem-1700	70	21	analyte	analyte	NOUN
eurjchem-1700	70	22	peak	peak	NOUN
eurjchem-1700	70	23	areas	area	NOUN
eurjchem-1700	70	24	of	of	ADP
eurjchem-1700	70	25	six	six	NUM
eurjchem-1700	70	26	replicate	replicate	ADJ
eurjchem-1700	70	27	injections	injection	NOUN
eurjchem-1700	70	28	less	less	ADJ
eurjchem-1700	70	29	than	than	ADP
eurjchem-1700	70	30	1	1	NUM
eurjchem-1700	70	31	%	%	NOUN
eurjchem-1700	70	32	was	be	AUX
eurjchem-1700	70	33	considered	consider	VERB
eurjchem-1700	70	34	to	to	PART
eurjchem-1700	70	35	be	be	AUX
eurjchem-1700	70	36	the	the	DET
eurjchem-1700	70	37	acceptance	acceptance	NOUN
eurjchem-1700	70	38	criteria	criterion	NOUN
eurjchem-1700	70	39	.	.	PUNCT
eurjchem-1700	71	1	2.5.2	2.5.2	NUM
eurjchem-1700	71	2	.	.	PUNCT
eurjchem-1700	71	3	linearity	linearity	NOUN
eurjchem-1700	71	4	linearity	linearity	NOUN
eurjchem-1700	71	5	of	of	ADP
eurjchem-1700	71	6	the	the	DET
eurjchem-1700	71	7	proposed	propose	VERB
eurjchem-1700	71	8	method	method	NOUN
eurjchem-1700	71	9	was	be	AUX
eurjchem-1700	71	10	evaluated	evaluate	VERB
eurjchem-1700	71	11	at	at	ADP
eurjchem-1700	71	12	five	five	NUM
eurjchem-1700	71	13	concentration	concentration	NOUN
eurjchem-1700	71	14	levels	level	NOUN
eurjchem-1700	71	15	in	in	ADP
eurjchem-1700	71	16	the	the	DET
eurjchem-1700	71	17	range	range	NOUN
eurjchem-1700	71	18	5	5	NUM
eurjchem-1700	71	19	to	to	PART
eurjchem-1700	71	20	50	50	NUM
eurjchem-1700	71	21	μg	μg	NOUN
eurjchem-1700	71	22	/	/	SYM
eurjchem-1700	71	23	ml	ml	PROPN
eurjchem-1700	71	24	.	.	PUNCT
eurjchem-1700	72	1	the	the	DET
eurjchem-1700	72	2	linearity	linearity	NOUN
eurjchem-1700	72	3	solutions	solution	NOUN
eurjchem-1700	72	4	were	be	AUX
eurjchem-1700	72	5	analysed	analyse	VERB
eurjchem-1700	72	6	in	in	ADP
eurjchem-1700	72	7	six	six	NUM
eurjchem-1700	72	8	replicates	replicate	NOUN
eurjchem-1700	72	9	and	and	CCONJ
eurjchem-1700	72	10	the	the	DET
eurjchem-1700	72	11	chromatograms	chromatogram	NOUN
eurjchem-1700	72	12	were	be	AUX
eurjchem-1700	72	13	recorded	record	VERB
eurjchem-1700	72	14	.	.	PUNCT
eurjchem-1700	73	1	calibration	calibration	NOUN
eurjchem-1700	73	2	plot	plot	NOUN
eurjchem-1700	73	3	was	be	AUX
eurjchem-1700	73	4	prepared	prepare	VERB
eurjchem-1700	73	5	by	by	ADP
eurjchem-1700	73	6	plotting	plot	VERB
eurjchem-1700	73	7	the	the	DET
eurjchem-1700	73	8	peak	peak	NOUN
eurjchem-1700	73	9	area	area	NOUN
eurjchem-1700	73	10	of	of	ADP
eurjchem-1700	73	11	analyte	analyte	NOUN
eurjchem-1700	73	12	against	against	ADP
eurjchem-1700	73	13	respective	respective	ADJ
eurjchem-1700	73	14	concentrations	concentration	NOUN
eurjchem-1700	73	15	and	and	CCONJ
eurjchem-1700	73	16	analysed	analyse	VERB
eurjchem-1700	73	17	by	by	ADP
eurjchem-1700	73	18	least	least	ADJ
eurjchem-1700	73	19	-	-	PUNCT
eurjchem-1700	73	20	square	square	NOUN
eurjchem-1700	73	21	regression	regression	NOUN
eurjchem-1700	73	22	;	;	PUNCT
eurjchem-1700	73	23	yintercept	yintercept	NOUN
eurjchem-1700	73	24	,	,	PUNCT
eurjchem-1700	73	25	slope	slope	NOUN
eurjchem-1700	73	26	and	and	CCONJ
eurjchem-1700	73	27	correlation	correlation	NOUN
eurjchem-1700	73	28	co	co	VERB
eurjchem-1700	73	29	-	-	ADJ
eurjchem-1700	73	30	efficient	efficient	ADJ
eurjchem-1700	73	31	were	be	AUX
eurjchem-1700	73	32	calculated	calculate	VERB
eurjchem-1700	73	33	.	.	PUNCT
eurjchem-1700	74	1	2.5.3	2.5.3	X
eurjchem-1700	74	2	.	.	PUNCT
eurjchem-1700	74	3	precision	precision	NOUN
eurjchem-1700	74	4	precision	precision	NOUN
eurjchem-1700	74	5	of	of	ADP
eurjchem-1700	74	6	the	the	DET
eurjchem-1700	74	7	developed	develop	VERB
eurjchem-1700	74	8	method	method	NOUN
eurjchem-1700	74	9	was	be	AUX
eurjchem-1700	74	10	assessed	assess	VERB
eurjchem-1700	74	11	by	by	ADP
eurjchem-1700	74	12	carrying	carry	VERB
eurjchem-1700	74	13	out	out	ADP
eurjchem-1700	74	14	the	the	DET
eurjchem-1700	74	15	assay	assay	ADJ
eurjchem-1700	74	16	analysis	analysis	NOUN
eurjchem-1700	74	17	of	of	ADP
eurjchem-1700	74	18	six	six	NUM
eurjchem-1700	74	19	independent	independent	ADJ
eurjchem-1700	74	20	cream	cream	NOUN
eurjchem-1700	74	21	samples	sample	NOUN
eurjchem-1700	74	22	at	at	ADP
eurjchem-1700	74	23	25	25	NUM
eurjchem-1700	74	24	μg	μg	NOUN
eurjchem-1700	74	25	/	/	SYM
eurjchem-1700	74	26	ml	ml	NOUN
eurjchem-1700	74	27	concentration	concentration	NOUN
eurjchem-1700	74	28	level	level	NOUN
eurjchem-1700	74	29	.	.	PUNCT
eurjchem-1700	75	1	to	to	PART
eurjchem-1700	75	2	assess	assess	VERB
eurjchem-1700	75	3	the	the	DET
eurjchem-1700	75	4	intraday	intraday	NOUN
eurjchem-1700	75	5	precision	precision	NOUN
eurjchem-1700	75	6	(	(	PUNCT
eurjchem-1700	75	7	repeatability	repeatability	NOUN
eurjchem-1700	75	8	)	)	PUNCT
eurjchem-1700	75	9	,	,	PUNCT
eurjchem-1700	75	10	the	the	DET
eurjchem-1700	75	11	%	%	NOUN
eurjchem-1700	75	12	rsd	rsd	NOUN
eurjchem-1700	75	13	of	of	ADP
eurjchem-1700	75	14	all	all	DET
eurjchem-1700	75	15	six	six	NUM
eurjchem-1700	75	16	samples	sample	NOUN
eurjchem-1700	75	17	analysed	analyse	VERB
eurjchem-1700	75	18	on	on	ADP
eurjchem-1700	75	19	the	the	DET
eurjchem-1700	75	20	same	same	ADJ
eurjchem-1700	75	21	day	day	NOUN
eurjchem-1700	75	22	on	on	ADP
eurjchem-1700	75	23	different	different	ADJ
eurjchem-1700	75	24	times	time	NOUN
eurjchem-1700	75	25	were	be	AUX
eurjchem-1700	75	26	calculated	calculate	VERB
eurjchem-1700	75	27	.	.	PUNCT
eurjchem-1700	76	1	inter	inter	ADJ
eurjchem-1700	76	2	-	-	ADJ
eurjchem-1700	76	3	day	day	ADJ
eurjchem-1700	76	4	precision	precision	NOUN
eurjchem-1700	76	5	was	be	AUX
eurjchem-1700	76	6	assessed	assess	VERB
eurjchem-1700	76	7	by	by	ADP
eurjchem-1700	76	8	analysing	analyse	VERB
eurjchem-1700	76	9	the	the	DET
eurjchem-1700	76	10	cream	cream	NOUN
eurjchem-1700	76	11	samples	sample	NOUN
eurjchem-1700	76	12	at	at	ADP
eurjchem-1700	76	13	different	different	ADJ
eurjchem-1700	76	14	days	day	NOUN
eurjchem-1700	76	15	by	by	ADP
eurjchem-1700	76	16	different	different	ADJ
eurjchem-1700	76	17	analyst	analyst	NOUN
eurjchem-1700	76	18	of	of	ADP
eurjchem-1700	76	19	the	the	DET
eurjchem-1700	76	20	same	same	ADJ
eurjchem-1700	76	21	laboratory	laboratory	NOUN
eurjchem-1700	76	22	.	.	PUNCT
eurjchem-1700	77	1	the	the	DET
eurjchem-1700	77	2	inter	inter	ADJ
eurjchem-1700	77	3	-	-	ADJ
eurjchem-1700	77	4	day	day	ADJ
eurjchem-1700	77	5	precision	precision	NOUN
eurjchem-1700	77	6	was	be	AUX
eurjchem-1700	77	7	expressed	express	VERB
eurjchem-1700	77	8	as	as	ADP
eurjchem-1700	77	9	%	%	NOUN
eurjchem-1700	77	10	rsd	rsd	NOUN
eurjchem-1700	77	11	of	of	ADP
eurjchem-1700	77	12	the	the	DET
eurjchem-1700	77	13	assay	assay	NOUN
eurjchem-1700	77	14	analysis	analysis	NOUN
eurjchem-1700	77	15	.	.	PUNCT
eurjchem-1700	78	1	2.5.4	2.5.4	NUM
eurjchem-1700	78	2	.	.	PUNCT
eurjchem-1700	78	3	accuracy	accuracy	NOUN
eurjchem-1700	78	4	accuracy	accuracy	NOUN
eurjchem-1700	78	5	of	of	ADP
eurjchem-1700	78	6	the	the	DET
eurjchem-1700	78	7	proposed	propose	VERB
eurjchem-1700	78	8	method	method	NOUN
eurjchem-1700	78	9	was	be	AUX
eurjchem-1700	78	10	estimated	estimate	VERB
eurjchem-1700	78	11	by	by	ADP
eurjchem-1700	78	12	performing	perform	VERB
eurjchem-1700	78	13	the	the	DET
eurjchem-1700	78	14	recovery	recovery	NOUN
eurjchem-1700	78	15	experiment	experiment	NOUN
eurjchem-1700	78	16	by	by	ADP
eurjchem-1700	78	17	following	follow	VERB
eurjchem-1700	78	18	standard	standard	ADJ
eurjchem-1700	78	19	addition	addition	NOUN
eurjchem-1700	78	20	procedure	procedure	NOUN
eurjchem-1700	78	21	.	.	PUNCT
eurjchem-1700	79	1	the	the	DET
eurjchem-1700	79	2	analysis	analysis	NOUN
eurjchem-1700	79	3	was	be	AUX
eurjchem-1700	79	4	carried	carry	VERB
eurjchem-1700	79	5	out	out	ADP
eurjchem-1700	79	6	by	by	ADP
eurjchem-1700	79	7	known	know	VERB
eurjchem-1700	79	8	2018	2018	NUM
eurjchem-1700	79	9	–	–	PUNCT
eurjchem-1700	79	10	european	european	ADJ
eurjchem-1700	79	11	journal	journal	NOUN
eurjchem-1700	79	12	of	of	ADP
eurjchem-1700	79	13	chemistry	chemistry	NOUN
eurjchem-1700	79	14	–	–	PUNCT
eurjchem-1700	79	15	cc	cc	NOUN
eurjchem-1700	79	16	by	by	ADP
eurjchem-1700	79	17	nc	nc	PROPN
eurjchem-1700	79	18	–	–	PUNCT
eurjchem-1700	79	19	doi	doi	PROPN
eurjchem-1700	79	20	:	:	PUNCT
eurjchem-1700	79	21	10.5155	10.5155	NUM
eurjchem-1700	79	22	/	/	SYM
eurjchem-1700	79	23	eurjchem.9.2.92	eurjchem.9.2.92	NOUN
eurjchem-1700	79	24	-	-	SYM
eurjchem-1700	79	25	98.1700	98.1700	NUM
eurjchem-1700	79	26	94	94	NUM
eurjchem-1700	79	27	alhazmi	alhazmi	PROPN
eurjchem-1700	79	28	et	et	NOUN
eurjchem-1700	79	29	al	al	PROPN
eurjchem-1700	79	30	.	.	PUNCT
eurjchem-1700	79	31	/	/	SYM
eurjchem-1700	79	32	european	european	PROPN
eurjchem-1700	79	33	journal	journal	PROPN
eurjchem-1700	79	34	of	of	ADP
eurjchem-1700	79	35	chemistry	chemistry	NOUN
eurjchem-1700	79	36	9	9	NUM
eurjchem-1700	79	37	(	(	PUNCT
eurjchem-1700	79	38	2	2	NUM
eurjchem-1700	79	39	)	)	PUNCT
eurjchem-1700	79	40	(	(	PUNCT
eurjchem-1700	79	41	2018	2018	NUM
eurjchem-1700	79	42	)	)	PUNCT
eurjchem-1700	79	43	92	92	NUM
eurjchem-1700	79	44	-	-	SYM
eurjchem-1700	79	45	98	98	NUM
eurjchem-1700	79	46	amount	amount	NOUN
eurjchem-1700	79	47	of	of	ADP
eurjchem-1700	79	48	clobetasone	clobetasone	NOUN
eurjchem-1700	79	49	butyrate	butyrate	NOUN
eurjchem-1700	79	50	working	working	PROPN
eurjchem-1700	79	51	standard	standard	NOUN
eurjchem-1700	79	52	added	add	VERB
eurjchem-1700	79	53	to	to	ADP
eurjchem-1700	79	54	pre	pre	ADJ
eurjchem-1700	79	55	-	-	ADJ
eurjchem-1700	79	56	analyzed	analyze	VERB
eurjchem-1700	79	57	solution	solution	NOUN
eurjchem-1700	79	58	of	of	ADP
eurjchem-1700	79	59	the	the	DET
eurjchem-1700	79	60	formulation	formulation	NOUN
eurjchem-1700	79	61	in	in	ADP
eurjchem-1700	79	62	the	the	DET
eurjchem-1700	79	63	test	test	NOUN
eurjchem-1700	79	64	concentration	concentration	NOUN
eurjchem-1700	79	65	range	range	NOUN
eurjchem-1700	79	66	of	of	ADP
eurjchem-1700	79	67	50	50	NUM
eurjchem-1700	79	68	,	,	PUNCT
eurjchem-1700	79	69	100	100	NUM
eurjchem-1700	79	70	and	and	CCONJ
eurjchem-1700	79	71	150	150	NUM
eurjchem-1700	79	72	%	%	NOUN
eurjchem-1700	79	73	.	.	PUNCT
eurjchem-1700	80	1	the	the	DET
eurjchem-1700	80	2	recovery	recovery	NOUN
eurjchem-1700	80	3	samples	sample	NOUN
eurjchem-1700	80	4	were	be	AUX
eurjchem-1700	80	5	run	run	VERB
eurjchem-1700	80	6	into	into	ADP
eurjchem-1700	80	7	the	the	DET
eurjchem-1700	80	8	hplc	hplc	NOUN
eurjchem-1700	80	9	system	system	NOUN
eurjchem-1700	80	10	in	in	ADP
eurjchem-1700	80	11	triplicate	triplicate	NOUN
eurjchem-1700	80	12	and	and	CCONJ
eurjchem-1700	80	13	mean	mean	VERB
eurjchem-1700	80	14	recovery	recovery	NOUN
eurjchem-1700	80	15	and	and	CCONJ
eurjchem-1700	80	16	%	%	NOUN
eurjchem-1700	80	17	rsd	rsd	PROPN
eurjchem-1700	80	18	were	be	AUX
eurjchem-1700	80	19	calculated	calculate	VERB
eurjchem-1700	80	20	.	.	PUNCT
eurjchem-1700	81	1	2.5.5	2.5.5	X
eurjchem-1700	81	2	.	.	X
eurjchem-1700	81	3	limit	limit	NOUN
eurjchem-1700	81	4	of	of	ADP
eurjchem-1700	81	5	detection	detection	NOUN
eurjchem-1700	81	6	and	and	CCONJ
eurjchem-1700	81	7	limit	limit	NOUN
eurjchem-1700	81	8	of	of	ADP
eurjchem-1700	81	9	quantitation	quantitation	NOUN
eurjchem-1700	81	10	the	the	DET
eurjchem-1700	81	11	limit	limit	NOUN
eurjchem-1700	81	12	of	of	ADP
eurjchem-1700	81	13	detection	detection	NOUN
eurjchem-1700	81	14	(	(	PUNCT
eurjchem-1700	81	15	lod	lod	PROPN
eurjchem-1700	81	16	)	)	PUNCT
eurjchem-1700	81	17	and	and	CCONJ
eurjchem-1700	81	18	limit	limit	NOUN
eurjchem-1700	81	19	of	of	ADP
eurjchem-1700	81	20	quantitation	quantitation	NOUN
eurjchem-1700	81	21	(	(	PUNCT
eurjchem-1700	81	22	loq	loq	PROPN
eurjchem-1700	81	23	)	)	PUNCT
eurjchem-1700	81	24	of	of	ADP
eurjchem-1700	81	25	the	the	DET
eurjchem-1700	81	26	present	present	ADJ
eurjchem-1700	81	27	method	method	NOUN
eurjchem-1700	81	28	were	be	AUX
eurjchem-1700	81	29	determined	determine	VERB
eurjchem-1700	81	30	by	by	ADP
eurjchem-1700	81	31	screening	screen	VERB
eurjchem-1700	81	32	a	a	DET
eurjchem-1700	81	33	series	series	NOUN
eurjchem-1700	81	34	of	of	ADP
eurjchem-1700	81	35	diluted	diluted	ADJ
eurjchem-1700	81	36	solutions	solution	NOUN
eurjchem-1700	81	37	of	of	ADP
eurjchem-1700	81	38	clobetasone	clobetasone	NOUN
eurjchem-1700	81	39	butyrate	butyrate	NOUN
eurjchem-1700	81	40	reference	reference	NOUN
eurjchem-1700	81	41	standard	standard	NOUN
eurjchem-1700	81	42	.	.	PUNCT
eurjchem-1700	82	1	the	the	DET
eurjchem-1700	82	2	solutions	solution	NOUN
eurjchem-1700	82	3	were	be	AUX
eurjchem-1700	82	4	prepared	prepare	VERB
eurjchem-1700	82	5	by	by	ADP
eurjchem-1700	82	6	sequentially	sequentially	ADV
eurjchem-1700	82	7	diluting	dilute	VERB
eurjchem-1700	82	8	the	the	DET
eurjchem-1700	82	9	standard	standard	ADJ
eurjchem-1700	82	10	solution	solution	NOUN
eurjchem-1700	82	11	in	in	ADP
eurjchem-1700	82	12	mobile	mobile	ADJ
eurjchem-1700	82	13	phase	phase	NOUN
eurjchem-1700	82	14	.	.	PUNCT
eurjchem-1700	83	1	the	the	DET
eurjchem-1700	83	2	lod	lod	PROPN
eurjchem-1700	83	3	and	and	CCONJ
eurjchem-1700	83	4	loq	loq	PROPN
eurjchem-1700	83	5	values	value	NOUN
eurjchem-1700	83	6	were	be	AUX
eurjchem-1700	83	7	calculated	calculate	VERB
eurjchem-1700	83	8	from	from	ADP
eurjchem-1700	83	9	signal	signal	NOUN
eurjchem-1700	83	10	-	-	PUNCT
eurjchem-1700	83	11	to	to	ADP
eurjchem-1700	83	12	-	-	PUNCT
eurjchem-1700	83	13	noise	noise	NOUN
eurjchem-1700	83	14	ratio	ratio	NOUN
eurjchem-1700	83	15	(	(	PUNCT
eurjchem-1700	83	16	s	s	NOUN
eurjchem-1700	83	17	/	/	SYM
eurjchem-1700	83	18	n	n	CCONJ
eurjchem-1700	83	19	)	)	PUNCT
eurjchem-1700	83	20	.	.	PUNCT
eurjchem-1700	84	1	the	the	DET
eurjchem-1700	84	2	lod	lod	PROPN
eurjchem-1700	84	3	value	value	NOUN
eurjchem-1700	84	4	for	for	ADP
eurjchem-1700	84	5	the	the	DET
eurjchem-1700	84	6	analyte	analyte	NOUN
eurjchem-1700	84	7	was	be	AUX
eurjchem-1700	84	8	considered	consider	VERB
eurjchem-1700	84	9	when	when	SCONJ
eurjchem-1700	84	10	s	s	X
eurjchem-1700	84	11	/	/	SYM
eurjchem-1700	84	12	n	n	NOUN
eurjchem-1700	84	13	=	=	SYM
eurjchem-1700	84	14	3	3	NUM
eurjchem-1700	84	15	and	and	CCONJ
eurjchem-1700	84	16	the	the	DET
eurjchem-1700	84	17	loq	loq	PROPN
eurjchem-1700	84	18	value	value	NOUN
eurjchem-1700	84	19	was	be	AUX
eurjchem-1700	84	20	evaluated	evaluate	VERB
eurjchem-1700	84	21	at	at	ADP
eurjchem-1700	84	22	s	s	PROPN
eurjchem-1700	84	23	/	/	SYM
eurjchem-1700	84	24	n	n	CCONJ
eurjchem-1700	84	25	=	=	SYM
eurjchem-1700	84	26	10	10	NUM
eurjchem-1700	84	27	criterion	criterion	NOUN
eurjchem-1700	84	28	.	.	PUNCT
eurjchem-1700	85	1	2.5.6	2.5.6	X
eurjchem-1700	85	2	.	.	PUNCT
eurjchem-1700	85	3	solution	solution	NOUN
eurjchem-1700	85	4	stability	stability	NOUN
eurjchem-1700	85	5	the	the	DET
eurjchem-1700	85	6	stability	stability	NOUN
eurjchem-1700	85	7	of	of	ADP
eurjchem-1700	85	8	the	the	DET
eurjchem-1700	85	9	tested	test	VERB
eurjchem-1700	85	10	drug	drug	NOUN
eurjchem-1700	85	11	in	in	ADP
eurjchem-1700	85	12	its	its	PRON
eurjchem-1700	85	13	analytical	analytical	ADJ
eurjchem-1700	85	14	solutions	solution	NOUN
eurjchem-1700	85	15	(	(	PUNCT
eurjchem-1700	85	16	standard	standard	ADJ
eurjchem-1700	85	17	and	and	CCONJ
eurjchem-1700	85	18	sample	sample	NOUN
eurjchem-1700	85	19	solutions	solution	NOUN
eurjchem-1700	85	20	)	)	PUNCT
eurjchem-1700	85	21	were	be	AUX
eurjchem-1700	85	22	tested	test	VERB
eurjchem-1700	85	23	by	by	ADP
eurjchem-1700	85	24	storing	store	VERB
eurjchem-1700	85	25	at	at	ADP
eurjchem-1700	85	26	laboratory	laboratory	NOUN
eurjchem-1700	85	27	temperature	temperature	NOUN
eurjchem-1700	85	28	(	(	PUNCT
eurjchem-1700	85	29	~25	~25	PROPN
eurjchem-1700	85	30	°	°	PROPN
eurjchem-1700	85	31	c	c	NOUN
eurjchem-1700	85	32	)	)	PUNCT
eurjchem-1700	85	33	for	for	ADP
eurjchem-1700	85	34	24	24	NUM
eurjchem-1700	85	35	hours	hour	NOUN
eurjchem-1700	85	36	and	and	CCONJ
eurjchem-1700	85	37	in	in	ADP
eurjchem-1700	85	38	the	the	DET
eurjchem-1700	85	39	refrigerator	refrigerator	NOUN
eurjchem-1700	85	40	(	(	PUNCT
eurjchem-1700	85	41	5±1	5±1	NUM
eurjchem-1700	85	42	°	°	NOUN
eurjchem-1700	85	43	c	c	NOUN
eurjchem-1700	85	44	)	)	PUNCT
eurjchem-1700	85	45	for	for	ADP
eurjchem-1700	85	46	72	72	NUM
eurjchem-1700	85	47	hours	hour	NOUN
eurjchem-1700	85	48	and	and	CCONJ
eurjchem-1700	85	49	analysing	analyse	VERB
eurjchem-1700	85	50	at	at	ADP
eurjchem-1700	85	51	12	12	NUM
eurjchem-1700	85	52	h	h	NOUN
eurjchem-1700	85	53	intervals	interval	NOUN
eurjchem-1700	85	54	.	.	PUNCT
eurjchem-1700	86	1	after	after	ADP
eurjchem-1700	86	2	every	every	DET
eurjchem-1700	86	3	12	12	NUM
eurjchem-1700	86	4	h	h	NOUN
eurjchem-1700	86	5	the	the	DET
eurjchem-1700	86	6	samples	sample	NOUN
eurjchem-1700	86	7	were	be	AUX
eurjchem-1700	86	8	analysed	analyse	VERB
eurjchem-1700	86	9	into	into	ADP
eurjchem-1700	86	10	the	the	DET
eurjchem-1700	86	11	hplc	hplc	NOUN
eurjchem-1700	86	12	system	system	NOUN
eurjchem-1700	86	13	in	in	ADP
eurjchem-1700	86	14	triplicate	triplicate	NOUN
eurjchem-1700	86	15	and	and	CCONJ
eurjchem-1700	86	16	the	the	DET
eurjchem-1700	86	17	assay	assay	NOUN
eurjchem-1700	86	18	results	result	NOUN
eurjchem-1700	86	19	were	be	AUX
eurjchem-1700	86	20	calculated	calculate	VERB
eurjchem-1700	86	21	from	from	ADP
eurjchem-1700	86	22	the	the	DET
eurjchem-1700	86	23	observed	observe	VERB
eurjchem-1700	86	24	peak	peak	NOUN
eurjchem-1700	86	25	area	area	NOUN
eurjchem-1700	86	26	.	.	PUNCT
eurjchem-1700	87	1	2.5.7	2.5.7	X
eurjchem-1700	87	2	.	.	X
eurjchem-1700	87	3	specificity	specificity	NOUN
eurjchem-1700	87	4	-	-	PUNCT
eurjchem-1700	87	5	forced	force	VERB
eurjchem-1700	87	6	degradation	degradation	NOUN
eurjchem-1700	87	7	studies	study	NOUN
eurjchem-1700	87	8	force	force	VERB
eurjchem-1700	87	9	degradation	degradation	NOUN
eurjchem-1700	87	10	studies	study	NOUN
eurjchem-1700	87	11	on	on	ADP
eurjchem-1700	87	12	the	the	DET
eurjchem-1700	87	13	clobetasone	clobetasone	NOUN
eurjchem-1700	87	14	butyrate	butyrate	NOUN
eurjchem-1700	87	15	cream	cream	NOUN
eurjchem-1700	87	16	sample	sample	NOUN
eurjchem-1700	87	17	was	be	AUX
eurjchem-1700	87	18	conducted	conduct	VERB
eurjchem-1700	87	19	to	to	PART
eurjchem-1700	87	20	reveal	reveal	VERB
eurjchem-1700	87	21	whether	whether	SCONJ
eurjchem-1700	87	22	the	the	DET
eurjchem-1700	87	23	developed	develop	VERB
eurjchem-1700	87	24	method	method	NOUN
eurjchem-1700	87	25	was	be	AUX
eurjchem-1700	87	26	possessing	possess	VERB
eurjchem-1700	87	27	stability	stability	NOUN
eurjchem-1700	87	28	-	-	PUNCT
eurjchem-1700	87	29	indicating	indicate	VERB
eurjchem-1700	87	30	property	property	NOUN
eurjchem-1700	87	31	and	and	CCONJ
eurjchem-1700	87	32	could	could	AUX
eurjchem-1700	87	33	unambiguously	unambiguously	ADV
eurjchem-1700	87	34	analyse	analyse	VERB
eurjchem-1700	87	35	the	the	DET
eurjchem-1700	87	36	test	test	NOUN
eurjchem-1700	87	37	drug	drug	NOUN
eurjchem-1700	87	38	in	in	ADP
eurjchem-1700	87	39	presence	presence	NOUN
eurjchem-1700	87	40	of	of	ADP
eurjchem-1700	87	41	degradation	degradation	NOUN
eurjchem-1700	87	42	products	product	NOUN
eurjchem-1700	87	43	and	and	CCONJ
eurjchem-1700	87	44	impurities	impurity	NOUN
eurjchem-1700	87	45	.	.	PUNCT
eurjchem-1700	88	1	the	the	DET
eurjchem-1700	88	2	clobetasone	clobetasone	NOUN
eurjchem-1700	88	3	butyrate	butyrate	NOUN
eurjchem-1700	88	4	cream	cream	NOUN
eurjchem-1700	88	5	sample	sample	NOUN
eurjchem-1700	88	6	was	be	AUX
eurjchem-1700	88	7	exposed	expose	VERB
eurjchem-1700	88	8	to	to	ADP
eurjchem-1700	88	9	stressed	stress	VERB
eurjchem-1700	88	10	conditions	condition	NOUN
eurjchem-1700	88	11	including	include	VERB
eurjchem-1700	88	12	acid	acid	NOUN
eurjchem-1700	88	13	hydrolysis	hydrolysis	NOUN
eurjchem-1700	88	14	,	,	PUNCT
eurjchem-1700	88	15	base	base	NOUN
eurjchem-1700	88	16	hydrolysis	hydrolysis	NOUN
eurjchem-1700	88	17	,	,	PUNCT
eurjchem-1700	88	18	oxidative	oxidative	ADJ
eurjchem-1700	88	19	stress	stress	NOUN
eurjchem-1700	88	20	,	,	PUNCT
eurjchem-1700	88	21	thermal	thermal	ADJ
eurjchem-1700	88	22	degradation	degradation	NOUN
eurjchem-1700	88	23	(	(	PUNCT
eurjchem-1700	88	24	dry	dry	ADJ
eurjchem-1700	88	25	and	and	CCONJ
eurjchem-1700	88	26	wet	wet	ADJ
eurjchem-1700	88	27	heat	heat	NOUN
eurjchem-1700	88	28	)	)	PUNCT
eurjchem-1700	88	29	and	and	CCONJ
eurjchem-1700	88	30	direct	direct	ADJ
eurjchem-1700	88	31	sunlight	sunlight	NOUN
eurjchem-1700	88	32	(	(	PUNCT
eurjchem-1700	88	33	photolytic	photolytic	ADJ
eurjchem-1700	88	34	degradation	degradation	NOUN
eurjchem-1700	88	35	)	)	PUNCT
eurjchem-1700	88	36	to	to	PART
eurjchem-1700	88	37	induce	induce	VERB
eurjchem-1700	88	38	partial	partial	ADJ
eurjchem-1700	88	39	degradation	degradation	NOUN
eurjchem-1700	88	40	of	of	ADP
eurjchem-1700	88	41	the	the	DET
eurjchem-1700	88	42	drug	drug	NOUN
eurjchem-1700	88	43	.	.	PUNCT
eurjchem-1700	89	1	acid	acid	ADJ
eurjchem-1700	89	2	degradation	degradation	NOUN
eurjchem-1700	89	3	:	:	PUNCT
eurjchem-1700	89	4	for	for	SCONJ
eurjchem-1700	89	5	acid	acid	NOUN
eurjchem-1700	89	6	degradation	degradation	NOUN
eurjchem-1700	89	7	study	study	NOUN
eurjchem-1700	89	8	the	the	DET
eurjchem-1700	89	9	cream	cream	NOUN
eurjchem-1700	89	10	sample	sample	NOUN
eurjchem-1700	89	11	was	be	AUX
eurjchem-1700	89	12	dispersed	disperse	VERB
eurjchem-1700	89	13	in	in	ADP
eurjchem-1700	89	14	10	10	NUM
eurjchem-1700	89	15	ml	ml	NOUN
eurjchem-1700	89	16	of	of	ADP
eurjchem-1700	89	17	diluent	diluent	NOUN
eurjchem-1700	89	18	and	and	CCONJ
eurjchem-1700	89	19	the	the	DET
eurjchem-1700	89	20	mixture	mixture	NOUN
eurjchem-1700	89	21	was	be	AUX
eurjchem-1700	89	22	subjected	subject	VERB
eurjchem-1700	89	23	to	to	ADP
eurjchem-1700	89	24	acid	acid	VERB
eurjchem-1700	89	25	hydrolysis	hydrolysis	NOUN
eurjchem-1700	89	26	by	by	ADP
eurjchem-1700	89	27	adding	add	VERB
eurjchem-1700	89	28	1	1	NUM
eurjchem-1700	89	29	ml	ml	NOUN
eurjchem-1700	89	30	of	of	ADP
eurjchem-1700	89	31	4	4	NUM
eurjchem-1700	89	32	n	n	PRON
eurjchem-1700	89	33	hcl	hcl	PROPN
eurjchem-1700	89	34	.	.	PUNCT
eurjchem-1700	90	1	the	the	DET
eurjchem-1700	90	2	resulting	result	VERB
eurjchem-1700	90	3	mixture	mixture	NOUN
eurjchem-1700	90	4	was	be	AUX
eurjchem-1700	90	5	left	leave	VERB
eurjchem-1700	90	6	in	in	ADP
eurjchem-1700	90	7	dark	dark	PROPN
eurjchem-1700	90	8	chamber	chamber	NOUN
eurjchem-1700	90	9	at	at	ADP
eurjchem-1700	90	10	37	37	NUM
eurjchem-1700	90	11	°	°	NOUN
eurjchem-1700	90	12	c	c	NOUN
eurjchem-1700	90	13	for	for	ADP
eurjchem-1700	90	14	1	1	NUM
eurjchem-1700	90	15	h.	h.	NOUN
eurjchem-1700	90	16	the	the	DET
eurjchem-1700	90	17	solution	solution	NOUN
eurjchem-1700	90	18	was	be	AUX
eurjchem-1700	90	19	then	then	ADV
eurjchem-1700	90	20	neutralized	neutralize	VERB
eurjchem-1700	90	21	with	with	ADP
eurjchem-1700	90	22	dilute	dilute	VERB
eurjchem-1700	90	23	naoh	naoh	NOUN
eurjchem-1700	90	24	solution	solution	NOUN
eurjchem-1700	90	25	.	.	PUNCT
eurjchem-1700	91	1	base	base	NOUN
eurjchem-1700	91	2	degradation	degradation	NOUN
eurjchem-1700	91	3	:	:	PUNCT
eurjchem-1700	91	4	for	for	SCONJ
eurjchem-1700	91	5	base	base	NOUN
eurjchem-1700	91	6	degradation	degradation	NOUN
eurjchem-1700	91	7	study	study	VERB
eurjchem-1700	91	8	the	the	DET
eurjchem-1700	91	9	cream	cream	NOUN
eurjchem-1700	91	10	sample	sample	NOUN
eurjchem-1700	91	11	was	be	AUX
eurjchem-1700	91	12	dispersed	disperse	VERB
eurjchem-1700	91	13	in	in	ADP
eurjchem-1700	91	14	10	10	NUM
eurjchem-1700	91	15	ml	ml	NOUN
eurjchem-1700	91	16	of	of	ADP
eurjchem-1700	91	17	diluent	diluent	NOUN
eurjchem-1700	91	18	and	and	CCONJ
eurjchem-1700	91	19	the	the	DET
eurjchem-1700	91	20	mixture	mixture	NOUN
eurjchem-1700	91	21	was	be	AUX
eurjchem-1700	91	22	subjected	subject	VERB
eurjchem-1700	91	23	to	to	PART
eurjchem-1700	91	24	base	base	VERB
eurjchem-1700	91	25	hydrolysis	hydrolysis	NOUN
eurjchem-1700	91	26	by	by	ADP
eurjchem-1700	91	27	adding	add	VERB
eurjchem-1700	91	28	1	1	NUM
eurjchem-1700	91	29	ml	ml	NOUN
eurjchem-1700	91	30	of	of	ADP
eurjchem-1700	91	31	1	1	NUM
eurjchem-1700	91	32	n	n	NOUN
eurjchem-1700	91	33	naoh	naoh	NOUN
eurjchem-1700	91	34	solution	solution	NOUN
eurjchem-1700	91	35	.	.	PUNCT
eurjchem-1700	92	1	the	the	DET
eurjchem-1700	92	2	resulting	result	VERB
eurjchem-1700	92	3	mixture	mixture	NOUN
eurjchem-1700	92	4	was	be	AUX
eurjchem-1700	92	5	kept	keep	VERB
eurjchem-1700	92	6	in	in	ADP
eurjchem-1700	92	7	dark	dark	ADJ
eurjchem-1700	92	8	chamber	chamber	NOUN
eurjchem-1700	92	9	at	at	ADP
eurjchem-1700	92	10	37	37	NUM
eurjchem-1700	92	11	°	°	NOUN
eurjchem-1700	92	12	c	c	NOUN
eurjchem-1700	92	13	for	for	ADP
eurjchem-1700	92	14	6	6	NUM
eurjchem-1700	92	15	h.	h.	NOUN
eurjchem-1700	92	16	the	the	DET
eurjchem-1700	92	17	solution	solution	NOUN
eurjchem-1700	92	18	was	be	AUX
eurjchem-1700	92	19	then	then	ADV
eurjchem-1700	92	20	neutralized	neutralize	VERB
eurjchem-1700	92	21	with	with	ADP
eurjchem-1700	92	22	dilute	dilute	PROPN
eurjchem-1700	92	23	hcl	hcl	PROPN
eurjchem-1700	92	24	.	.	PUNCT
eurjchem-1700	93	1	oxidative	oxidative	ADJ
eurjchem-1700	93	2	degradation	degradation	NOUN
eurjchem-1700	93	3	:	:	PUNCT
eurjchem-1700	93	4	to	to	PART
eurjchem-1700	93	5	examine	examine	VERB
eurjchem-1700	93	6	the	the	DET
eurjchem-1700	93	7	stability	stability	NOUN
eurjchem-1700	93	8	of	of	ADP
eurjchem-1700	93	9	the	the	DET
eurjchem-1700	93	10	test	test	NOUN
eurjchem-1700	93	11	drug	drug	NOUN
eurjchem-1700	93	12	towards	towards	ADP
eurjchem-1700	93	13	oxidation	oxidation	NOUN
eurjchem-1700	93	14	,	,	PUNCT
eurjchem-1700	93	15	the	the	DET
eurjchem-1700	93	16	weighed	weigh	VERB
eurjchem-1700	93	17	cream	cream	NOUN
eurjchem-1700	93	18	sample	sample	NOUN
eurjchem-1700	93	19	was	be	AUX
eurjchem-1700	93	20	dispersed	disperse	VERB
eurjchem-1700	93	21	with	with	ADP
eurjchem-1700	93	22	10	10	NUM
eurjchem-1700	93	23	ml	ml	NOUN
eurjchem-1700	93	24	of	of	ADP
eurjchem-1700	93	25	diluent	diluent	NOUN
eurjchem-1700	93	26	and	and	CCONJ
eurjchem-1700	93	27	the	the	DET
eurjchem-1700	93	28	oxidation	oxidation	NOUN
eurjchem-1700	93	29	was	be	AUX
eurjchem-1700	93	30	accomplished	accomplish	VERB
eurjchem-1700	93	31	by	by	ADP
eurjchem-1700	93	32	addition	addition	NOUN
eurjchem-1700	93	33	of	of	ADP
eurjchem-1700	93	34	1	1	NUM
eurjchem-1700	93	35	ml	ml	NOUN
eurjchem-1700	93	36	of	of	ADP
eurjchem-1700	93	37	30	30	NUM
eurjchem-1700	93	38	%	%	NOUN
eurjchem-1700	93	39	hydrogen	hydrogen	NOUN
eurjchem-1700	93	40	peroxide	peroxide	NOUN
eurjchem-1700	93	41	.	.	PUNCT
eurjchem-1700	94	1	the	the	DET
eurjchem-1700	94	2	resulting	result	VERB
eurjchem-1700	94	3	mixture	mixture	NOUN
eurjchem-1700	94	4	was	be	AUX
eurjchem-1700	94	5	kept	keep	VERB
eurjchem-1700	94	6	in	in	ADP
eurjchem-1700	94	7	dark	dark	ADJ
eurjchem-1700	94	8	chamber	chamber	NOUN
eurjchem-1700	94	9	for	for	ADP
eurjchem-1700	94	10	6	6	NUM
eurjchem-1700	94	11	h	h	NOUN
eurjchem-1700	94	12	at	at	ADP
eurjchem-1700	94	13	37	37	NUM
eurjchem-1700	94	14	°	°	NOUN
eurjchem-1700	94	15	c	c	NOUN
eurjchem-1700	94	16	.	.	PUNCT
eurjchem-1700	95	1	thermal	thermal	ADJ
eurjchem-1700	95	2	degradation	degradation	NOUN
eurjchem-1700	95	3	:	:	PUNCT
eurjchem-1700	95	4	the	the	DET
eurjchem-1700	95	5	thermal	thermal	ADJ
eurjchem-1700	95	6	degradation	degradation	NOUN
eurjchem-1700	95	7	was	be	AUX
eurjchem-1700	95	8	examined	examine	VERB
eurjchem-1700	95	9	at	at	ADP
eurjchem-1700	95	10	wet	wet	ADJ
eurjchem-1700	95	11	heat	heat	NOUN
eurjchem-1700	95	12	conditions	condition	NOUN
eurjchem-1700	95	13	.	.	PUNCT
eurjchem-1700	96	1	the	the	DET
eurjchem-1700	96	2	sample	sample	NOUN
eurjchem-1700	96	3	was	be	AUX
eurjchem-1700	96	4	dispersed	disperse	VERB
eurjchem-1700	96	5	in	in	ADP
eurjchem-1700	96	6	5	5	NUM
eurjchem-1700	96	7	ml	ml	ADP
eurjchem-1700	96	8	ultra	ultra	ADJ
eurjchem-1700	96	9	-	-	ADJ
eurjchem-1700	96	10	pure	pure	ADJ
eurjchem-1700	96	11	water	water	NOUN
eurjchem-1700	96	12	and	and	CCONJ
eurjchem-1700	96	13	heated	heat	VERB
eurjchem-1700	96	14	on	on	ADP
eurjchem-1700	96	15	water	water	NOUN
eurjchem-1700	96	16	bath	bath	NOUN
eurjchem-1700	96	17	(	(	PUNCT
eurjchem-1700	96	18	~100	~100	PROPN
eurjchem-1700	96	19	°	°	NOUN
eurjchem-1700	96	20	c	c	NOUN
eurjchem-1700	96	21	)	)	PUNCT
eurjchem-1700	96	22	for	for	ADP
eurjchem-1700	96	23	6	6	NUM
eurjchem-1700	96	24	h.	h.	PROPN
eurjchem-1700	96	25	photolytic	photolytic	ADJ
eurjchem-1700	96	26	degradation	degradation	NOUN
eurjchem-1700	96	27	:	:	PUNCT
eurjchem-1700	96	28	to	to	PART
eurjchem-1700	96	29	examine	examine	VERB
eurjchem-1700	96	30	the	the	DET
eurjchem-1700	96	31	photostability	photostability	NOUN
eurjchem-1700	96	32	of	of	ADP
eurjchem-1700	96	33	the	the	DET
eurjchem-1700	96	34	clobetasone	clobetasone	NOUN
eurjchem-1700	96	35	cream	cream	NOUN
eurjchem-1700	96	36	,	,	PUNCT
eurjchem-1700	96	37	the	the	DET
eurjchem-1700	96	38	sample	sample	NOUN
eurjchem-1700	96	39	was	be	AUX
eurjchem-1700	96	40	exposed	expose	VERB
eurjchem-1700	96	41	to	to	ADP
eurjchem-1700	96	42	direct	direct	ADJ
eurjchem-1700	96	43	sunlight	sunlight	NOUN
eurjchem-1700	96	44	for	for	ADP
eurjchem-1700	96	45	6	6	NUM
eurjchem-1700	96	46	h.	h.	NOUN
eurjchem-1700	96	47	all	all	DET
eurjchem-1700	96	48	the	the	DET
eurjchem-1700	96	49	forced	force	VERB
eurjchem-1700	96	50	degradation	degradation	NOUN
eurjchem-1700	96	51	experiments	experiment	NOUN
eurjchem-1700	96	52	were	be	AUX
eurjchem-1700	96	53	carried	carry	VERB
eurjchem-1700	96	54	out	out	ADP
eurjchem-1700	96	55	at	at	ADP
eurjchem-1700	96	56	a	a	DET
eurjchem-1700	96	57	concentration	concentration	NOUN
eurjchem-1700	96	58	of	of	ADP
eurjchem-1700	96	59	25	25	NUM
eurjchem-1700	96	60	μg	μg	NOUN
eurjchem-1700	96	61	/	/	SYM
eurjchem-1700	96	62	ml	ml	NOUN
eurjchem-1700	96	63	.	.	PUNCT
eurjchem-1700	97	1	in	in	ADP
eurjchem-1700	97	2	all	all	DET
eurjchem-1700	97	3	the	the	DET
eurjchem-1700	97	4	experiments	experiment	NOUN
eurjchem-1700	97	5	clobetasone	clobetasone	VERB
eurjchem-1700	97	6	butyrate	butyrate	ADJ
eurjchem-1700	97	7	cream	cream	NOUN
eurjchem-1700	97	8	content	content	NOUN
eurjchem-1700	97	9	equivalent	equivalent	ADJ
eurjchem-1700	97	10	to	to	ADP
eurjchem-1700	97	11	5	5	NUM
eurjchem-1700	97	12	mg	mg	NOUN
eurjchem-1700	97	13	of	of	ADP
eurjchem-1700	97	14	clobetasone	clobetasone	NOUN
eurjchem-1700	97	15	butyrate	butyrate	NOUN
eurjchem-1700	97	16	was	be	AUX
eurjchem-1700	97	17	weighed	weigh	VERB
eurjchem-1700	97	18	and	and	CCONJ
eurjchem-1700	97	19	the	the	DET
eurjchem-1700	97	20	samples	sample	NOUN
eurjchem-1700	97	21	solutions	solution	NOUN
eurjchem-1700	97	22	were	be	AUX
eurjchem-1700	97	23	prepared	prepare	VERB
eurjchem-1700	97	24	by	by	ADP
eurjchem-1700	97	25	following	follow	VERB
eurjchem-1700	97	26	the	the	DET
eurjchem-1700	97	27	same	same	ADJ
eurjchem-1700	97	28	procedure	procedure	NOUN
eurjchem-1700	97	29	as	as	SCONJ
eurjchem-1700	97	30	described	describe	VERB
eurjchem-1700	97	31	in	in	ADP
eurjchem-1700	97	32	the	the	DET
eurjchem-1700	97	33	sample	sample	NOUN
eurjchem-1700	97	34	preparation	preparation	NOUN
eurjchem-1700	97	35	section	section	NOUN
eurjchem-1700	97	36	.	.	PUNCT
eurjchem-1700	98	1	all	all	DET
eurjchem-1700	98	2	the	the	DET
eurjchem-1700	98	3	degradation	degradation	NOUN
eurjchem-1700	98	4	experiments	experiment	NOUN
eurjchem-1700	98	5	were	be	AUX
eurjchem-1700	98	6	performed	perform	VERB
eurjchem-1700	98	7	in	in	ADP
eurjchem-1700	98	8	four	four	NUM
eurjchem-1700	98	9	replicates	replicate	NOUN
eurjchem-1700	98	10	.	.	PUNCT
eurjchem-1700	99	1	the	the	DET
eurjchem-1700	99	2	sample	sample	NOUN
eurjchem-1700	99	3	solutions	solution	NOUN
eurjchem-1700	99	4	were	be	AUX
eurjchem-1700	99	5	injected	inject	VERB
eurjchem-1700	99	6	in	in	ADP
eurjchem-1700	99	7	triplicate	triplicate	NOUN
eurjchem-1700	99	8	in	in	ADP
eurjchem-1700	99	9	the	the	DET
eurjchem-1700	99	10	hplc	hplc	NOUN
eurjchem-1700	99	11	system	system	NOUN
eurjchem-1700	99	12	using	use	VERB
eurjchem-1700	99	13	the	the	DET
eurjchem-1700	99	14	developed	develop	VERB
eurjchem-1700	99	15	method	method	NOUN
eurjchem-1700	99	16	and	and	CCONJ
eurjchem-1700	99	17	chromatograms	chromatogram	NOUN
eurjchem-1700	99	18	were	be	AUX
eurjchem-1700	99	19	recorded	record	VERB
eurjchem-1700	99	20	.	.	PUNCT
eurjchem-1700	100	1	peak	peak	NOUN
eurjchem-1700	100	2	purity	purity	NOUN
eurjchem-1700	100	3	of	of	ADP
eurjchem-1700	100	4	the	the	DET
eurjchem-1700	100	5	main	main	ADJ
eurjchem-1700	100	6	analyte	analyte	NOUN
eurjchem-1700	100	7	peak	peak	NOUN
eurjchem-1700	100	8	was	be	AUX
eurjchem-1700	100	9	checked	check	VERB
eurjchem-1700	100	10	by	by	ADP
eurjchem-1700	100	11	pda	pda	NOUN
eurjchem-1700	100	12	detector	detector	NOUN
eurjchem-1700	100	13	and	and	CCONJ
eurjchem-1700	100	14	the	the	DET
eurjchem-1700	100	15	assay	assay	NOUN
eurjchem-1700	100	16	results	result	NOUN
eurjchem-1700	100	17	were	be	AUX
eurjchem-1700	100	18	calculated	calculate	VERB
eurjchem-1700	100	19	against	against	ADP
eurjchem-1700	100	20	the	the	DET
eurjchem-1700	100	21	reference	reference	NOUN
eurjchem-1700	100	22	standard	standard	NOUN
eurjchem-1700	100	23	.	.	PUNCT
eurjchem-1700	101	1	3	3	X
eurjchem-1700	101	2	.	.	NOUN
eurjchem-1700	101	3	results	result	NOUN
eurjchem-1700	101	4	and	and	CCONJ
eurjchem-1700	101	5	discussion	discussion	NOUN
eurjchem-1700	101	6	3.1	3.1	NUM
eurjchem-1700	101	7	.	.	PUNCT
eurjchem-1700	101	8	method	method	NOUN
eurjchem-1700	101	9	development	development	NOUN
eurjchem-1700	101	10	and	and	CCONJ
eurjchem-1700	101	11	optimization	optimization	NOUN
eurjchem-1700	101	12	the	the	DET
eurjchem-1700	101	13	major	major	ADJ
eurjchem-1700	101	14	objective	objective	NOUN
eurjchem-1700	101	15	of	of	ADP
eurjchem-1700	101	16	the	the	DET
eurjchem-1700	101	17	current	current	ADJ
eurjchem-1700	101	18	study	study	NOUN
eurjchem-1700	101	19	was	be	AUX
eurjchem-1700	101	20	to	to	PART
eurjchem-1700	101	21	develop	develop	VERB
eurjchem-1700	101	22	a	a	DET
eurjchem-1700	101	23	simple	simple	ADJ
eurjchem-1700	101	24	,	,	PUNCT
eurjchem-1700	101	25	sensitive	sensitive	ADJ
eurjchem-1700	101	26	and	and	CCONJ
eurjchem-1700	101	27	accurate	accurate	ADJ
eurjchem-1700	101	28	reversed	reverse	VERB
eurjchem-1700	101	29	-	-	PUNCT
eurjchem-1700	101	30	phase	phase	NOUN
eurjchem-1700	101	31	hplc	hplc	NOUN
eurjchem-1700	101	32	method	method	NOUN
eurjchem-1700	101	33	for	for	ADP
eurjchem-1700	101	34	determination	determination	NOUN
eurjchem-1700	101	35	clobetasone	clobetasone	NOUN
eurjchem-1700	101	36	butyrate	butyrate	NOUN
eurjchem-1700	101	37	in	in	ADP
eurjchem-1700	101	38	bulk	bulk	ADJ
eurjchem-1700	101	39	and	and	CCONJ
eurjchem-1700	101	40	cream	cream	ADJ
eurjchem-1700	101	41	formulation	formulation	NOUN
eurjchem-1700	101	42	.	.	PUNCT
eurjchem-1700	102	1	the	the	DET
eurjchem-1700	102	2	aim	aim	NOUN
eurjchem-1700	102	3	was	be	AUX
eurjchem-1700	102	4	also	also	ADV
eurjchem-1700	102	5	to	to	PART
eurjchem-1700	102	6	separate	separate	VERB
eurjchem-1700	102	7	the	the	DET
eurjchem-1700	102	8	degradation	degradation	NOUN
eurjchem-1700	102	9	products	product	NOUN
eurjchem-1700	102	10	of	of	ADP
eurjchem-1700	102	11	the	the	DET
eurjchem-1700	102	12	test	test	NOUN
eurjchem-1700	102	13	drug	drug	NOUN
eurjchem-1700	102	14	in	in	ADP
eurjchem-1700	102	15	a	a	DET
eurjchem-1700	102	16	short	short	ADJ
eurjchem-1700	102	17	runtime	runtime	NOUN
eurjchem-1700	102	18	.	.	PUNCT
eurjchem-1700	103	1	in	in	ADP
eurjchem-1700	103	2	the	the	DET
eurjchem-1700	103	3	development	development	NOUN
eurjchem-1700	103	4	process	process	NOUN
eurjchem-1700	103	5	,	,	PUNCT
eurjchem-1700	103	6	various	various	ADJ
eurjchem-1700	103	7	buffers	buffer	NOUN
eurjchem-1700	103	8	and	and	CCONJ
eurjchem-1700	103	9	ph	ph	ADJ
eurjchem-1700	103	10	range	range	NOUN
eurjchem-1700	103	11	of	of	ADP
eurjchem-1700	103	12	4	4	NUM
eurjchem-1700	103	13	-	-	SYM
eurjchem-1700	103	14	8	8	NUM
eurjchem-1700	103	15	and	and	CCONJ
eurjchem-1700	103	16	composition	composition	NOUN
eurjchem-1700	103	17	of	of	ADP
eurjchem-1700	103	18	aqueous	aqueous	ADJ
eurjchem-1700	103	19	and	and	CCONJ
eurjchem-1700	103	20	organic	organic	ADJ
eurjchem-1700	103	21	phases	phase	NOUN
eurjchem-1700	103	22	were	be	AUX
eurjchem-1700	103	23	tried	try	VERB
eurjchem-1700	103	24	.	.	PUNCT
eurjchem-1700	104	1	two	two	NUM
eurjchem-1700	104	2	organic	organic	ADJ
eurjchem-1700	104	3	solvents	solvent	NOUN
eurjchem-1700	104	4	,	,	PUNCT
eurjchem-1700	104	5	acetonitrile	acetonitrile	NOUN
eurjchem-1700	104	6	and	and	CCONJ
eurjchem-1700	104	7	methanol	methanol	NOUN
eurjchem-1700	104	8	were	be	AUX
eurjchem-1700	104	9	tested	test	VERB
eurjchem-1700	104	10	.	.	PUNCT
eurjchem-1700	105	1	methanol	methanol	NOUN
eurjchem-1700	105	2	was	be	AUX
eurjchem-1700	105	3	found	find	VERB
eurjchem-1700	105	4	to	to	PART
eurjchem-1700	105	5	be	be	AUX
eurjchem-1700	105	6	superior	superior	ADJ
eurjchem-1700	105	7	in	in	ADP
eurjchem-1700	105	8	terms	term	NOUN
eurjchem-1700	105	9	of	of	ADP
eurjchem-1700	105	10	chromategraphic	chromategraphic	ADJ
eurjchem-1700	105	11	characteristic	characteristic	NOUN
eurjchem-1700	105	12	of	of	ADP
eurjchem-1700	105	13	the	the	DET
eurjchem-1700	105	14	tested	test	VERB
eurjchem-1700	105	15	drug	drug	NOUN
eurjchem-1700	105	16	.	.	PUNCT
eurjchem-1700	106	1	after	after	ADP
eurjchem-1700	106	2	several	several	ADJ
eurjchem-1700	106	3	trials	trial	NOUN
eurjchem-1700	106	4	,	,	PUNCT
eurjchem-1700	106	5	a	a	DET
eurjchem-1700	106	6	mixture	mixture	NOUN
eurjchem-1700	106	7	of	of	ADP
eurjchem-1700	106	8	methanol	methanol	NOUN
eurjchem-1700	106	9	and	and	CCONJ
eurjchem-1700	106	10	water	water	NOUN
eurjchem-1700	106	11	at	at	ADP
eurjchem-1700	106	12	a	a	DET
eurjchem-1700	106	13	ratio	ratio	NOUN
eurjchem-1700	106	14	of	of	ADP
eurjchem-1700	106	15	84:16	84:16	NUM
eurjchem-1700	106	16	(	(	PUNCT
eurjchem-1700	106	17	v	v	NOUN
eurjchem-1700	106	18	:	:	PUNCT
eurjchem-1700	106	19	v	v	NOUN
eurjchem-1700	106	20	)	)	PUNCT
eurjchem-1700	106	21	(	(	PUNCT
eurjchem-1700	106	22	ph	ph	NOUN
eurjchem-1700	106	23	=	=	NOUN
eurjchem-1700	106	24	6.0	6.0	NUM
eurjchem-1700	106	25	)	)	PUNCT
eurjchem-1700	106	26	was	be	AUX
eurjchem-1700	106	27	found	find	VERB
eurjchem-1700	106	28	to	to	PART
eurjchem-1700	106	29	be	be	AUX
eurjchem-1700	106	30	optimum	optimum	ADJ
eurjchem-1700	106	31	for	for	ADP
eurjchem-1700	106	32	the	the	DET
eurjchem-1700	106	33	developed	develop	VERB
eurjchem-1700	106	34	method	method	NOUN
eurjchem-1700	106	35	.	.	PUNCT
eurjchem-1700	107	1	at	at	ADP
eurjchem-1700	107	2	a	a	DET
eurjchem-1700	107	3	mobile	mobile	ADJ
eurjchem-1700	107	4	phase	phase	NOUN
eurjchem-1700	107	5	composition	composition	NOUN
eurjchem-1700	107	6	of	of	ADP
eurjchem-1700	107	7	methanol	methanol	NOUN
eurjchem-1700	107	8	and	and	CCONJ
eurjchem-1700	107	9	water	water	NOUN
eurjchem-1700	107	10	(	(	PUNCT
eurjchem-1700	107	11	50:50	50:50	NUM
eurjchem-1700	107	12	,	,	PUNCT
eurjchem-1700	107	13	v	v	NOUN
eurjchem-1700	107	14	:	:	SYM
eurjchem-1700	107	15	v	v	NOUN
eurjchem-1700	107	16	,	,	PUNCT
eurjchem-1700	107	17	ph	ph	NOUN
eurjchem-1700	107	18	=	=	NOUN
eurjchem-1700	107	19	6.0	6.0	NUM
eurjchem-1700	107	20	)	)	PUNCT
eurjchem-1700	107	21	,	,	PUNCT
eurjchem-1700	107	22	no	no	DET
eurjchem-1700	107	23	analyte	analyte	NOUN
eurjchem-1700	107	24	peak	peak	NOUN
eurjchem-1700	107	25	was	be	AUX
eurjchem-1700	107	26	observed	observe	VERB
eurjchem-1700	107	27	within	within	ADP
eurjchem-1700	107	28	10	10	NUM
eurjchem-1700	107	29	min	min	NOUN
eurjchem-1700	107	30	runtime	runtime	NOUN
eurjchem-1700	107	31	.	.	PUNCT
eurjchem-1700	108	1	hence	hence	ADV
eurjchem-1700	108	2	,	,	PUNCT
eurjchem-1700	108	3	the	the	DET
eurjchem-1700	108	4	proportion	proportion	NOUN
eurjchem-1700	108	5	of	of	ADP
eurjchem-1700	108	6	methanol	methanol	NOUN
eurjchem-1700	108	7	was	be	AUX
eurjchem-1700	108	8	gradually	gradually	ADV
eurjchem-1700	108	9	increased	increase	VERB
eurjchem-1700	108	10	until	until	SCONJ
eurjchem-1700	108	11	the	the	DET
eurjchem-1700	108	12	drug	drug	NOUN
eurjchem-1700	108	13	has	have	AUX
eurjchem-1700	108	14	been	be	AUX
eurjchem-1700	108	15	eluted	elute	VERB
eurjchem-1700	108	16	at	at	ADP
eurjchem-1700	108	17	about	about	ADV
eurjchem-1700	108	18	4	4	NUM
eurjchem-1700	108	19	min	min	NOUN
eurjchem-1700	108	20	at	at	ADP
eurjchem-1700	108	21	1	1	NUM
eurjchem-1700	108	22	ml	ml	NOUN
eurjchem-1700	108	23	/	/	SYM
eurjchem-1700	108	24	min	min	NOUN
eurjchem-1700	108	25	flow	flow	NOUN
eurjchem-1700	108	26	rate	rate	NOUN
eurjchem-1700	108	27	.	.	PUNCT
eurjchem-1700	109	1	a	a	DET
eurjchem-1700	109	2	detection	detection	NOUN
eurjchem-1700	109	3	wavelength	wavelength	NOUN
eurjchem-1700	109	4	of	of	ADP
eurjchem-1700	109	5	240	240	NUM
eurjchem-1700	109	6	nm	nm	NOUN
eurjchem-1700	109	7	was	be	AUX
eurjchem-1700	109	8	selected	select	VERB
eurjchem-1700	109	9	on	on	ADP
eurjchem-1700	109	10	the	the	DET
eurjchem-1700	109	11	basis	basis	NOUN
eurjchem-1700	109	12	of	of	ADP
eurjchem-1700	109	13	uv	uv	NOUN
eurjchem-1700	109	14	-	-	PUNCT
eurjchem-1700	109	15	spectral	spectral	ADJ
eurjchem-1700	109	16	scanning	scanning	NOUN
eurjchem-1700	109	17	of	of	ADP
eurjchem-1700	109	18	the	the	DET
eurjchem-1700	109	19	standard	standard	ADJ
eurjchem-1700	109	20	solution	solution	NOUN
eurjchem-1700	109	21	.	.	PUNCT
eurjchem-1700	110	1	based	base	VERB
eurjchem-1700	110	2	on	on	ADP
eurjchem-1700	110	3	results	result	NOUN
eurjchem-1700	110	4	obtained	obtain	VERB
eurjchem-1700	110	5	from	from	ADP
eurjchem-1700	110	6	several	several	ADJ
eurjchem-1700	110	7	trails	trail	NOUN
eurjchem-1700	110	8	during	during	ADP
eurjchem-1700	110	9	the	the	DET
eurjchem-1700	110	10	method	method	NOUN
eurjchem-1700	110	11	optimization	optimization	NOUN
eurjchem-1700	110	12	step	step	NOUN
eurjchem-1700	110	13	,	,	PUNCT
eurjchem-1700	110	14	c18	c18	NOUN
eurjchem-1700	110	15	column	column	NOUN
eurjchem-1700	110	16	(	(	PUNCT
eurjchem-1700	110	17	50	50	NUM
eurjchem-1700	110	18	mm	mm	NOUN
eurjchem-1700	110	19	×	×	NOUN
eurjchem-1700	110	20	4.6	4.6	NUM
eurjchem-1700	110	21	mm	mm	NOUN
eurjchem-1700	110	22	,	,	PUNCT
eurjchem-1700	110	23	5	5	NUM
eurjchem-1700	110	24	μm	μm	NOUN
eurjchem-1700	110	25	)	)	PUNCT
eurjchem-1700	110	26	was	be	AUX
eurjchem-1700	110	27	found	find	VERB
eurjchem-1700	110	28	to	to	PART
eurjchem-1700	110	29	be	be	AUX
eurjchem-1700	110	30	optimum	optimum	ADJ
eurjchem-1700	110	31	stationary	stationary	ADJ
eurjchem-1700	110	32	phase	phase	NOUN
eurjchem-1700	110	33	.	.	PUNCT
eurjchem-1700	111	1	other	other	ADJ
eurjchem-1700	111	2	parameters	parameter	NOUN
eurjchem-1700	111	3	such	such	ADJ
eurjchem-1700	111	4	as	as	ADP
eurjchem-1700	111	5	injection	injection	NOUN
eurjchem-1700	111	6	volume	volume	NOUN
eurjchem-1700	111	7	of	of	ADP
eurjchem-1700	111	8	20	20	NUM
eurjchem-1700	111	9	μl	μl	ADV
eurjchem-1700	111	10	and	and	CCONJ
eurjchem-1700	111	11	column	column	NOUN
eurjchem-1700	111	12	oven	oven	VERB
eurjchem-1700	111	13	temperature	temperature	NOUN
eurjchem-1700	111	14	of	of	ADP
eurjchem-1700	111	15	27	27	NUM
eurjchem-1700	111	16	°	°	NOUN
eurjchem-1700	111	17	c	c	NOUN
eurjchem-1700	111	18	were	be	AUX
eurjchem-1700	111	19	also	also	ADV
eurjchem-1700	111	20	optimized	optimize	VERB
eurjchem-1700	111	21	.	.	PUNCT
eurjchem-1700	112	1	by	by	ADP
eurjchem-1700	112	2	applying	apply	VERB
eurjchem-1700	112	3	the	the	DET
eurjchem-1700	112	4	finalized	finalized	ADJ
eurjchem-1700	112	5	chromatographic	chromatographic	ADJ
eurjchem-1700	112	6	conditions	condition	NOUN
eurjchem-1700	112	7	,	,	PUNCT
eurjchem-1700	112	8	the	the	DET
eurjchem-1700	112	9	standard	standard	NOUN
eurjchem-1700	112	10	and	and	CCONJ
eurjchem-1700	112	11	sample	sample	NOUN
eurjchem-1700	112	12	solutions	solution	NOUN
eurjchem-1700	112	13	were	be	AUX
eurjchem-1700	112	14	analysed	analyse	VERB
eurjchem-1700	112	15	.	.	PUNCT
eurjchem-1700	113	1	the	the	DET
eurjchem-1700	113	2	representative	representative	ADJ
eurjchem-1700	113	3	chromatograms	chromatogram	NOUN
eurjchem-1700	113	4	of	of	ADP
eurjchem-1700	113	5	clobetasone	clobetasone	NOUN
eurjchem-1700	113	6	butyrate	butyrate	NOUN
eurjchem-1700	113	7	in	in	ADP
eurjchem-1700	113	8	bulk	bulk	ADJ
eurjchem-1700	113	9	and	and	CCONJ
eurjchem-1700	113	10	cream	cream	NOUN
eurjchem-1700	113	11	formulation	formulation	NOUN
eurjchem-1700	113	12	showing	show	VERB
eurjchem-1700	113	13	excellent	excellent	ADJ
eurjchem-1700	113	14	peak	peak	NOUN
eurjchem-1700	113	15	shape	shape	NOUN
eurjchem-1700	113	16	have	have	AUX
eurjchem-1700	113	17	been	be	AUX
eurjchem-1700	113	18	depicted	depict	VERB
eurjchem-1700	113	19	in	in	ADP
eurjchem-1700	113	20	figure	figure	NOUN
eurjchem-1700	113	21	2	2	NUM
eurjchem-1700	113	22	.	.	PUNCT
eurjchem-1700	114	1	the	the	DET
eurjchem-1700	114	2	extraction	extraction	NOUN
eurjchem-1700	114	3	and	and	CCONJ
eurjchem-1700	114	4	good	good	ADJ
eurjchem-1700	114	5	recovery	recovery	NOUN
eurjchem-1700	114	6	of	of	ADP
eurjchem-1700	114	7	the	the	DET
eurjchem-1700	114	8	active	active	ADJ
eurjchem-1700	114	9	drug	drug	NOUN
eurjchem-1700	114	10	from	from	ADP
eurjchem-1700	114	11	a	a	DET
eurjchem-1700	114	12	semisolid	semisolid	NOUN
eurjchem-1700	114	13	matrix	matrix	NOUN
eurjchem-1700	114	14	such	such	ADJ
eurjchem-1700	114	15	as	as	ADP
eurjchem-1700	114	16	cream	cream	NOUN
eurjchem-1700	114	17	is	be	AUX
eurjchem-1700	114	18	one	one	NUM
eurjchem-1700	114	19	of	of	ADP
eurjchem-1700	114	20	the	the	DET
eurjchem-1700	114	21	critical	critical	ADJ
eurjchem-1700	114	22	aspects	aspect	NOUN
eurjchem-1700	114	23	of	of	ADP
eurjchem-1700	114	24	analysing	analyse	VERB
eurjchem-1700	114	25	semisolid	semisolid	NOUN
eurjchem-1700	114	26	dosage	dosage	NOUN
eurjchem-1700	114	27	forms	form	NOUN
eurjchem-1700	114	28	.	.	PUNCT
eurjchem-1700	115	1	hence	hence	ADV
eurjchem-1700	115	2	,	,	PUNCT
eurjchem-1700	115	3	considering	consider	VERB
eurjchem-1700	115	4	the	the	DET
eurjchem-1700	115	5	solubility	solubility	NOUN
eurjchem-1700	115	6	of	of	ADP
eurjchem-1700	115	7	clobetasone	clobetasone	NOUN
eurjchem-1700	115	8	butyrate	butyrate	NOUN
eurjchem-1700	115	9	,	,	PUNCT
eurjchem-1700	115	10	mobile	mobile	ADJ
eurjchem-1700	115	11	phase	phase	NOUN
eurjchem-1700	115	12	(	(	PUNCT
eurjchem-1700	115	13	methanol	methanol	NOUN
eurjchem-1700	115	14	:	:	PUNCT
eurjchem-1700	115	15	water	water	NOUN
eurjchem-1700	115	16	,	,	PUNCT
eurjchem-1700	115	17	84:16	84:16	NUM
eurjchem-1700	115	18	,	,	PUNCT
eurjchem-1700	115	19	v	v	ADP
eurjchem-1700	115	20	:	:	SYM
eurjchem-1700	115	21	v	v	NOUN
eurjchem-1700	115	22	,	,	PUNCT
eurjchem-1700	115	23	ph	ph	NOUN
eurjchem-1700	115	24	=	=	NOUN
eurjchem-1700	115	25	6.0	6.0	NUM
eurjchem-1700	115	26	)	)	PUNCT
eurjchem-1700	115	27	was	be	AUX
eurjchem-1700	115	28	used	use	VERB
eurjchem-1700	115	29	as	as	ADP
eurjchem-1700	115	30	diluent	diluent	NOUN
eurjchem-1700	115	31	for	for	ADP
eurjchem-1700	115	32	the	the	DET
eurjchem-1700	115	33	preparation	preparation	NOUN
eurjchem-1700	115	34	and	and	CCONJ
eurjchem-1700	115	35	dilution	dilution	NOUN
eurjchem-1700	115	36	of	of	ADP
eurjchem-1700	115	37	all	all	DET
eurjchem-1700	115	38	analytical	analytical	ADJ
eurjchem-1700	115	39	solutions	solution	NOUN
eurjchem-1700	115	40	.	.	PUNCT
eurjchem-1700	116	1	3.2	3.2	NUM
eurjchem-1700	116	2	.	.	PUNCT
eurjchem-1700	116	3	method	method	NOUN
eurjchem-1700	116	4	validation	validation	NOUN
eurjchem-1700	116	5	after	after	ADP
eurjchem-1700	116	6	finalizing	finalize	VERB
eurjchem-1700	116	7	the	the	DET
eurjchem-1700	116	8	optimum	optimum	ADJ
eurjchem-1700	116	9	chromatographic	chromatographic	ADJ
eurjchem-1700	116	10	conditions	condition	NOUN
eurjchem-1700	116	11	,	,	PUNCT
eurjchem-1700	116	12	the	the	DET
eurjchem-1700	116	13	method	method	NOUN
eurjchem-1700	116	14	was	be	AUX
eurjchem-1700	116	15	subjected	subject	VERB
eurjchem-1700	116	16	to	to	ADP
eurjchem-1700	116	17	validation	validation	NOUN
eurjchem-1700	116	18	according	accord	VERB
eurjchem-1700	116	19	to	to	ADP
eurjchem-1700	116	20	ich	ich	PROPN
eurjchem-1700	116	21	guidelines	guideline	NOUN
eurjchem-1700	116	22	q2	q2	NOUN
eurjchem-1700	116	23	r1	r1	PROPN
eurjchem-1700	117	1	[	[	X
eurjchem-1700	117	2	14	14	NUM
eurjchem-1700	117	3	]	]	PUNCT
eurjchem-1700	117	4	.	.	PUNCT
eurjchem-1700	118	1	the	the	DET
eurjchem-1700	118	2	developed	develop	VERB
eurjchem-1700	118	3	method	method	NOUN
eurjchem-1700	118	4	has	have	AUX
eurjchem-1700	118	5	been	be	AUX
eurjchem-1700	118	6	evaluated	evaluate	VERB
eurjchem-1700	118	7	for	for	ADP
eurjchem-1700	118	8	system	system	NOUN
eurjchem-1700	118	9	suitability	suitability	NOUN
eurjchem-1700	118	10	,	,	PUNCT
eurjchem-1700	118	11	linearity	linearity	NOUN
eurjchem-1700	118	12	,	,	PUNCT
eurjchem-1700	118	13	precision	precision	NOUN
eurjchem-1700	118	14	,	,	PUNCT
eurjchem-1700	118	15	accuracy	accuracy	NOUN
eurjchem-1700	118	16	,	,	PUNCT
eurjchem-1700	118	17	sensitivity	sensitivity	NOUN
eurjchem-1700	118	18	,	,	PUNCT
eurjchem-1700	118	19	solution	solution	NOUN
eurjchem-1700	118	20	stability	stability	NOUN
eurjchem-1700	118	21	and	and	CCONJ
eurjchem-1700	118	22	specificity	specificity	NOUN
eurjchem-1700	118	23	.	.	PUNCT
eurjchem-1700	119	1	the	the	DET
eurjchem-1700	119	2	system	system	NOUN
eurjchem-1700	119	3	suitability	suitability	NOUN
eurjchem-1700	119	4	and	and	CCONJ
eurjchem-1700	119	5	column	column	NOUN
eurjchem-1700	119	6	performance	performance	NOUN
eurjchem-1700	119	7	were	be	AUX
eurjchem-1700	119	8	demonstrated	demonstrate	VERB
eurjchem-1700	119	9	by	by	ADP
eurjchem-1700	119	10	injecting	inject	VERB
eurjchem-1700	119	11	standard	standard	ADJ
eurjchem-1700	119	12	solution	solution	NOUN
eurjchem-1700	119	13	at	at	ADP
eurjchem-1700	119	14	the	the	DET
eurjchem-1700	119	15	beginning	beginning	NOUN
eurjchem-1700	119	16	of	of	ADP
eurjchem-1700	119	17	the	the	DET
eurjchem-1700	119	18	experiment	experiment	NOUN
eurjchem-1700	119	19	and	and	CCONJ
eurjchem-1700	119	20	the	the	DET
eurjchem-1700	119	21	system	system	NOUN
eurjchem-1700	119	22	suitability	suitability	NOUN
eurjchem-1700	119	23	parameters	parameter	NOUN
eurjchem-1700	119	24	were	be	AUX
eurjchem-1700	119	25	recorded	record	VERB
eurjchem-1700	119	26	form	form	NOUN
eurjchem-1700	119	27	the	the	DET
eurjchem-1700	119	28	chromatograms	chromatogram	NOUN
eurjchem-1700	119	29	.	.	PUNCT
eurjchem-1700	120	1	the	the	DET
eurjchem-1700	120	2	tailing	tail	VERB
eurjchem-1700	120	3	factor	factor	NOUN
eurjchem-1700	120	4	for	for	ADP
eurjchem-1700	120	5	clobetasone	clobetasone	NOUN
eurjchem-1700	120	6	butyrate	butyrate	NOUN
eurjchem-1700	120	7	peak	peak	NOUN
eurjchem-1700	120	8	was	be	AUX
eurjchem-1700	120	9	0.99	0.99	NUM
eurjchem-1700	120	10	and	and	CCONJ
eurjchem-1700	120	11	number	number	NOUN
eurjchem-1700	120	12	of	of	ADP
eurjchem-1700	120	13	theoretical	theoretical	ADJ
eurjchem-1700	120	14	plates	plate	NOUN
eurjchem-1700	120	15	was	be	AUX
eurjchem-1700	120	16	recorded	record	VERB
eurjchem-1700	120	17	to	to	PART
eurjchem-1700	120	18	be	be	AUX
eurjchem-1700	120	19	4986	4986	NUM
eurjchem-1700	120	20	,	,	PUNCT
eurjchem-1700	120	21	which	which	PRON
eurjchem-1700	120	22	has	have	AUX
eurjchem-1700	120	23	verified	verify	VERB
eurjchem-1700	120	24	the	the	DET
eurjchem-1700	120	25	column	column	NOUN
eurjchem-1700	120	26	efficiency	efficiency	NOUN
eurjchem-1700	120	27	.	.	PUNCT
eurjchem-1700	121	1	the	the	DET
eurjchem-1700	121	2	%	%	NOUN
eurjchem-1700	121	3	relative	relative	ADJ
eurjchem-1700	121	4	standard	standard	ADJ
eurjchem-1700	121	5	deviation	deviation	NOUN
eurjchem-1700	121	6	(	(	PUNCT
eurjchem-1700	121	7	rsd	rsd	NOUN
eurjchem-1700	121	8	)	)	PUNCT
eurjchem-1700	121	9	of	of	ADP
eurjchem-1700	121	10	the	the	DET
eurjchem-1700	121	11	peak	peak	NOUN
eurjchem-1700	121	12	area	area	NOUN
eurjchem-1700	121	13	of	of	ADP
eurjchem-1700	121	14	six	six	NUM
eurjchem-1700	121	15	replicate	replicate	ADJ
eurjchem-1700	121	16	injections	injection	NOUN
eurjchem-1700	121	17	was	be	AUX
eurjchem-1700	121	18	0.42	0.42	NUM
eurjchem-1700	121	19	,	,	PUNCT
eurjchem-1700	121	20	which	which	PRON
eurjchem-1700	121	21	has	have	AUX
eurjchem-1700	121	22	indicated	indicate	VERB
eurjchem-1700	121	23	that	that	SCONJ
eurjchem-1700	121	24	the	the	DET
eurjchem-1700	121	25	hplc	hplc	NOUN
eurjchem-1700	121	26	system	system	NOUN
eurjchem-1700	121	27	was	be	AUX
eurjchem-1700	121	28	precise	precise	ADJ
eurjchem-1700	121	29	.	.	PUNCT
eurjchem-1700	122	1	the	the	DET
eurjchem-1700	122	2	acceptable	acceptable	ADJ
eurjchem-1700	122	3	system	system	NOUN
eurjchem-1700	122	4	suitability	suitability	NOUN
eurjchem-1700	122	5	parameters	parameter	NOUN
eurjchem-1700	122	6	have	have	AUX
eurjchem-1700	122	7	suggested	suggest	VERB
eurjchem-1700	122	8	that	that	SCONJ
eurjchem-1700	122	9	the	the	DET
eurjchem-1700	122	10	system	system	NOUN
eurjchem-1700	122	11	was	be	AUX
eurjchem-1700	122	12	suitable	suitable	ADJ
eurjchem-1700	122	13	to	to	PART
eurjchem-1700	122	14	conduct	conduct	VERB
eurjchem-1700	122	15	the	the	DET
eurjchem-1700	122	16	experiment	experiment	NOUN
eurjchem-1700	122	17	.	.	PUNCT
eurjchem-1700	123	1	the	the	DET
eurjchem-1700	123	2	system	system	NOUN
eurjchem-1700	123	3	suitability	suitability	NOUN
eurjchem-1700	123	4	parameters	parameter	NOUN
eurjchem-1700	123	5	were	be	AUX
eurjchem-1700	123	6	monitored	monitor	VERB
eurjchem-1700	123	7	throughout	throughout	ADP
eurjchem-1700	123	8	the	the	DET
eurjchem-1700	123	9	experiment	experiment	NOUN
eurjchem-1700	123	10	.	.	PUNCT
eurjchem-1700	124	1	to	to	PART
eurjchem-1700	124	2	demonstrate	demonstrate	VERB
eurjchem-1700	124	3	the	the	DET
eurjchem-1700	124	4	linearity	linearity	NOUN
eurjchem-1700	124	5	of	of	ADP
eurjchem-1700	124	6	the	the	DET
eurjchem-1700	124	7	developed	develop	VERB
eurjchem-1700	124	8	hplc	hplc	NOUN
eurjchem-1700	124	9	method	method	NOUN
eurjchem-1700	124	10	,	,	PUNCT
eurjchem-1700	124	11	the	the	DET
eurjchem-1700	124	12	standard	standard	ADJ
eurjchem-1700	124	13	solutions	solution	NOUN
eurjchem-1700	124	14	over	over	ADP
eurjchem-1700	124	15	the	the	DET
eurjchem-1700	124	16	concentration	concentration	NOUN
eurjchem-1700	124	17	range	range	NOUN
eurjchem-1700	124	18	of	of	ADP
eurjchem-1700	124	19	5	5	NUM
eurjchem-1700	124	20	to	to	PART
eurjchem-1700	124	21	50	50	NUM
eurjchem-1700	124	22	μg	μg	NOUN
eurjchem-1700	124	23	/	/	SYM
eurjchem-1700	124	24	ml	ml	NOUN
eurjchem-1700	124	25	at	at	ADP
eurjchem-1700	124	26	five	five	NUM
eurjchem-1700	124	27	point	point	NOUN
eurjchem-1700	124	28	levels	level	NOUN
eurjchem-1700	124	29	were	be	AUX
eurjchem-1700	124	30	analysed	analyse	VERB
eurjchem-1700	124	31	.	.	PUNCT
eurjchem-1700	125	1	the	the	DET
eurjchem-1700	125	2	linear	linear	ADJ
eurjchem-1700	125	3	calibration	calibration	NOUN
eurjchem-1700	125	4	graph	graph	NOUN
eurjchem-1700	125	5	was	be	AUX
eurjchem-1700	125	6	obtained	obtain	VERB
eurjchem-1700	125	7	between	between	ADP
eurjchem-1700	125	8	the	the	DET
eurjchem-1700	125	9	observed	observe	VERB
eurjchem-1700	125	10	peak	peak	NOUN
eurjchem-1700	125	11	areas	area	NOUN
eurjchem-1700	125	12	of	of	ADP
eurjchem-1700	125	13	analyte	analyte	NOUN
eurjchem-1700	125	14	and	and	CCONJ
eurjchem-1700	125	15	the	the	DET
eurjchem-1700	125	16	concentration	concentration	NOUN
eurjchem-1700	125	17	of	of	ADP
eurjchem-1700	125	18	the	the	DET
eurjchem-1700	125	19	respective	respective	ADJ
eurjchem-1700	125	20	linearity	linearity	NOUN
eurjchem-1700	125	21	solutions	solution	NOUN
eurjchem-1700	125	22	(	(	PUNCT
eurjchem-1700	125	23	figure	figure	NOUN
eurjchem-1700	125	24	3	3	NUM
eurjchem-1700	125	25	)	)	PUNCT
eurjchem-1700	125	26	.	.	PUNCT
eurjchem-1700	126	1	2018	2018	NUM
eurjchem-1700	126	2	–	–	PUNCT
eurjchem-1700	126	3	european	european	ADJ
eurjchem-1700	126	4	journal	journal	NOUN
eurjchem-1700	126	5	of	of	ADP
eurjchem-1700	126	6	chemistry	chemistry	NOUN
eurjchem-1700	126	7	–	–	PUNCT
eurjchem-1700	126	8	cc	cc	NOUN
eurjchem-1700	126	9	by	by	ADP
eurjchem-1700	126	10	nc	nc	PROPN
eurjchem-1700	126	11	–	–	PUNCT
eurjchem-1700	126	12	doi	doi	PROPN
eurjchem-1700	126	13	:	:	PUNCT
eurjchem-1700	126	14	10.5155	10.5155	NUM
eurjchem-1700	126	15	/	/	SYM
eurjchem-1700	126	16	eurjchem.9.2.92	eurjchem.9.2.92	NOUN
eurjchem-1700	126	17	-	-	SYM
eurjchem-1700	126	18	98.1700	98.1700	NUM
eurjchem-1700	126	19	alhazmi	alhazmi	NOUN
eurjchem-1700	126	20	et	et	NOUN
eurjchem-1700	126	21	al	al	PROPN
eurjchem-1700	126	22	.	.	PUNCT
eurjchem-1700	126	23	/	/	SYM
eurjchem-1700	126	24	european	european	PROPN
eurjchem-1700	126	25	journal	journal	PROPN
eurjchem-1700	126	26	of	of	ADP
eurjchem-1700	126	27	chemistry	chemistry	NOUN
eurjchem-1700	126	28	9	9	NUM
eurjchem-1700	126	29	(	(	PUNCT
eurjchem-1700	126	30	2	2	NUM
eurjchem-1700	126	31	)	)	PUNCT
eurjchem-1700	126	32	(	(	PUNCT
eurjchem-1700	126	33	2018	2018	NUM
eurjchem-1700	126	34	)	)	PUNCT
eurjchem-1700	126	35	92	92	NUM
eurjchem-1700	126	36	-	-	SYM
eurjchem-1700	126	37	98	98	NUM
eurjchem-1700	126	38	95	95	NUM
eurjchem-1700	126	39	table	table	NOUN
eurjchem-1700	126	40	1	1	NUM
eurjchem-1700	126	41	.	.	PUNCT
eurjchem-1700	127	1	linearity	linearity	NOUN
eurjchem-1700	127	2	results	result	NOUN
eurjchem-1700	127	3	of	of	ADP
eurjchem-1700	127	4	clobetasone	clobetasone	NOUN
eurjchem-1700	127	5	butyrate	butyrate	NOUN
eurjchem-1700	127	6	by	by	ADP
eurjchem-1700	127	7	the	the	DET
eurjchem-1700	127	8	proposed	propose	VERB
eurjchem-1700	127	9	hplc	hplc	NOUN
eurjchem-1700	127	10	method	method	NOUN
eurjchem-1700	127	11	*	*	PUNCT
eurjchem-1700	127	12	.	.	PUNCT
eurjchem-1700	128	1	parameters	parameter	NOUN
eurjchem-1700	128	2	clobetasone	clobetasone	VERB
eurjchem-1700	128	3	butyrate	butyrate	NOUN
eurjchem-1700	128	4	linearity	linearity	PROPN
eurjchem-1700	128	5	range	range	NOUN
eurjchem-1700	128	6	(	(	PUNCT
eurjchem-1700	128	7	μg	μg	NOUN
eurjchem-1700	128	8	/	/	SYM
eurjchem-1700	128	9	ml	ml	NOUN
eurjchem-1700	128	10	)	)	PUNCT
eurjchem-1700	128	11	5	5	NUM
eurjchem-1700	128	12	-	-	SYM
eurjchem-1700	128	13	50	50	NUM
eurjchem-1700	128	14	correlation	correlation	NOUN
eurjchem-1700	128	15	coefficient	coefficient	NOUN
eurjchem-1700	128	16	(	(	PUNCT
eurjchem-1700	128	17	r2	r2	PROPN
eurjchem-1700	128	18	)	)	PUNCT
eurjchem-1700	128	19	0.9993	0.9993	NUM
eurjchem-1700	128	20	slope	slope	NOUN
eurjchem-1700	128	21	(	(	PUNCT
eurjchem-1700	128	22	a	a	NOUN
eurjchem-1700	128	23	)	)	PUNCT
eurjchem-1700	128	24	150.2	150.2	NUM
eurjchem-1700	128	25	intercept	intercept	NOUN
eurjchem-1700	128	26	(	(	PUNCT
eurjchem-1700	128	27	b	b	NOUN
eurjchem-1700	128	28	)	)	PUNCT
eurjchem-1700	128	29	2151.3	2151.3	NUM
eurjchem-1700	128	30	regression	regression	NOUN
eurjchem-1700	128	31	equation	equation	NOUN
eurjchem-1700	128	32	(	(	PUNCT
eurjchem-1700	128	33	y	y	NOUN
eurjchem-1700	128	34	=	=	NOUN
eurjchem-1700	128	35	ax	ax	NOUN
eurjchem-1700	128	36	+	+	CCONJ
eurjchem-1700	128	37	b	b	X
eurjchem-1700	128	38	)	)	PUNCT
eurjchem-1700	128	39	y	y	NOUN
eurjchem-1700	128	40	=	=	PUNCT
eurjchem-1700	128	41	150.2x	150.2x	NUM
eurjchem-1700	128	42	+	+	CCONJ
eurjchem-1700	128	43	2151.3	2151.3	NUM
eurjchem-1700	128	44	*	*	NOUN
eurjchem-1700	128	45	the	the	DET
eurjchem-1700	128	46	linearity	linearity	NOUN
eurjchem-1700	128	47	solutions	solution	NOUN
eurjchem-1700	128	48	were	be	AUX
eurjchem-1700	128	49	injected	inject	VERB
eurjchem-1700	128	50	in	in	ADP
eurjchem-1700	128	51	six	six	NUM
eurjchem-1700	128	52	replicates	replicate	NOUN
eurjchem-1700	128	53	table	table	NOUN
eurjchem-1700	128	54	2	2	NUM
eurjchem-1700	128	55	.	.	PUNCT
eurjchem-1700	128	56	standard	standard	ADJ
eurjchem-1700	128	57	deviation	deviation	NOUN
eurjchem-1700	128	58	and	and	CCONJ
eurjchem-1700	128	59	%	%	NOUN
eurjchem-1700	128	60	relative	relative	ADJ
eurjchem-1700	128	61	standard	standard	ADJ
eurjchem-1700	128	62	deviation	deviation	NOUN
eurjchem-1700	128	63	of	of	ADP
eurjchem-1700	128	64	the	the	DET
eurjchem-1700	128	65	peak	peak	NOUN
eurjchem-1700	128	66	area	area	NOUN
eurjchem-1700	128	67	of	of	ADP
eurjchem-1700	128	68	recorded	record	VERB
eurjchem-1700	128	69	in	in	ADP
eurjchem-1700	128	70	linearity	linearity	NOUN
eurjchem-1700	128	71	experiment	experiment	NOUN
eurjchem-1700	128	72	(	(	PUNCT
eurjchem-1700	128	73	n	n	NOUN
eurjchem-1700	128	74	=	=	SYM
eurjchem-1700	128	75	6	6	NUM
eurjchem-1700	128	76	)	)	PUNCT
eurjchem-1700	128	77	.	.	PUNCT
eurjchem-1700	129	1	concentrations	concentration	NOUN
eurjchem-1700	129	2	(	(	PUNCT
eurjchem-1700	129	3	μg	μg	NOUN
eurjchem-1700	129	4	/	/	SYM
eurjchem-1700	129	5	ml	ml	NOUN
eurjchem-1700	129	6	)	)	PUNCT
eurjchem-1700	129	7	standard	standard	ADJ
eurjchem-1700	129	8	deviation	deviation	NOUN
eurjchem-1700	129	9	(	(	PUNCT
eurjchem-1700	129	10	sd	sd	NOUN
eurjchem-1700	129	11	)	)	PUNCT
eurjchem-1700	129	12	%	%	NOUN
eurjchem-1700	129	13	relative	relative	ADJ
eurjchem-1700	129	14	standard	standard	ADJ
eurjchem-1700	129	15	deviation	deviation	NOUN
eurjchem-1700	129	16	(	(	PUNCT
eurjchem-1700	129	17	%	%	INTJ
eurjchem-1700	129	18	rsd	rsd	NOUN
eurjchem-1700	129	19	)	)	PUNCT
eurjchem-1700	129	20	5	5	NUM
eurjchem-1700	129	21	30.97	30.97	NUM
eurjchem-1700	129	22	1.08	1.08	NUM
eurjchem-1700	129	23	10	10	NUM
eurjchem-1700	129	24	33.19	33.19	NUM
eurjchem-1700	129	25	0.92	0.92	NUM
eurjchem-1700	129	26	20	20	NUM
eurjchem-1700	129	27	35.49	35.49	NUM
eurjchem-1700	129	28	0.67	0.67	NUM
eurjchem-1700	129	29	25	25	NUM
eurjchem-1700	129	30	31.03	31.03	NUM
eurjchem-1700	129	31	0.53	0.53	NUM
eurjchem-1700	129	32	50	50	NUM
eurjchem-1700	129	33	40.72	40.72	NUM
eurjchem-1700	129	34	0.42	0.42	NUM
eurjchem-1700	129	35	(	(	PUNCT
eurjchem-1700	129	36	a	a	NOUN
eurjchem-1700	129	37	)	)	PUNCT
eurjchem-1700	129	38	(	(	PUNCT
eurjchem-1700	129	39	b	b	X
eurjchem-1700	129	40	)	)	PUNCT
eurjchem-1700	129	41	figure	figure	NOUN
eurjchem-1700	129	42	2	2	NUM
eurjchem-1700	129	43	.	.	PUNCT
eurjchem-1700	129	44	representative	representative	ADJ
eurjchem-1700	129	45	chromatograms	chromatogram	NOUN
eurjchem-1700	129	46	of	of	ADP
eurjchem-1700	129	47	clobetasone	clobetasone	NOUN
eurjchem-1700	129	48	butyrate	butyrate	NOUN
eurjchem-1700	129	49	in	in	ADP
eurjchem-1700	129	50	standard	standard	PROPN
eurjchem-1700	129	51	(	(	PUNCT
eurjchem-1700	129	52	a	a	NOUN
eurjchem-1700	129	53	)	)	PUNCT
eurjchem-1700	129	54	and	and	CCONJ
eurjchem-1700	129	55	cream	cream	NOUN
eurjchem-1700	129	56	sample	sample	NOUN
eurjchem-1700	129	57	(	(	PUNCT
eurjchem-1700	129	58	b	b	NOUN
eurjchem-1700	129	59	)	)	PUNCT
eurjchem-1700	129	60	.	.	PUNCT
eurjchem-1700	130	1	0	0	NUM
eurjchem-1700	131	1	2000	2000	NUM
eurjchem-1700	131	2	4000	4000	NUM
eurjchem-1700	131	3	6000	6000	NUM
eurjchem-1700	131	4	8000	8000	NUM
eurjchem-1700	131	5	10000	10000	NUM
eurjchem-1700	131	6	12000	12000	NUM
eurjchem-1700	131	7	0	0	NUM
eurjchem-1700	131	8	10	10	NUM
eurjchem-1700	131	9	20	20	NUM
eurjchem-1700	131	10	30	30	NUM
eurjchem-1700	131	11	40	40	NUM
eurjchem-1700	131	12	50	50	NUM
eurjchem-1700	131	13	60	60	NUM
eurjchem-1700	131	14	pe	pe	PROPN
eurjchem-1700	131	15	ak	ak	PROPN
eurjchem-1700	131	16	a	a	PRON
eurjchem-1700	131	17	re	re	X
eurjchem-1700	131	18	a	a	DET
eurjchem-1700	131	19	(	(	PUNCT
eurjchem-1700	131	20	a	a	DET
eurjchem-1700	131	21	u	u	NOUN
eurjchem-1700	131	22	)	)	PUNCT
eurjchem-1700	131	23	concentration	concentration	NOUN
eurjchem-1700	131	24	(	(	PUNCT
eurjchem-1700	131	25	μg	μg	NOUN
eurjchem-1700	131	26	/	/	SYM
eurjchem-1700	131	27	ml	ml	NOUN
eurjchem-1700	131	28	)	)	PUNCT
eurjchem-1700	131	29	figure	figure	NOUN
eurjchem-1700	131	30	3	3	NUM
eurjchem-1700	131	31	.	.	PUNCT
eurjchem-1700	131	32	calibration	calibration	NOUN
eurjchem-1700	131	33	graph	graph	NOUN
eurjchem-1700	131	34	of	of	ADP
eurjchem-1700	131	35	clobetasone	clobetasone	NOUN
eurjchem-1700	131	36	butyrate	butyrate	NOUN
eurjchem-1700	131	37	.	.	PUNCT
eurjchem-1700	132	1	the	the	DET
eurjchem-1700	132	2	regression	regression	NOUN
eurjchem-1700	132	3	analysis	analysis	NOUN
eurjchem-1700	132	4	showed	show	VERB
eurjchem-1700	132	5	the	the	DET
eurjchem-1700	132	6	existence	existence	NOUN
eurjchem-1700	132	7	of	of	ADP
eurjchem-1700	132	8	an	an	DET
eurjchem-1700	132	9	excellent	excellent	ADJ
eurjchem-1700	132	10	correlation	correlation	NOUN
eurjchem-1700	132	11	between	between	ADP
eurjchem-1700	132	12	the	the	DET
eurjchem-1700	132	13	observed	observe	VERB
eurjchem-1700	132	14	peak	peak	NOUN
eurjchem-1700	132	15	area	area	NOUN
eurjchem-1700	132	16	and	and	CCONJ
eurjchem-1700	132	17	concentration	concentration	NOUN
eurjchem-1700	132	18	of	of	ADP
eurjchem-1700	132	19	the	the	DET
eurjchem-1700	132	20	analyte	analyte	NOUN
eurjchem-1700	132	21	,	,	PUNCT
eurjchem-1700	132	22	which	which	PRON
eurjchem-1700	132	23	has	have	AUX
eurjchem-1700	132	24	proved	prove	VERB
eurjchem-1700	132	25	the	the	DET
eurjchem-1700	132	26	linearity	linearity	NOUN
eurjchem-1700	132	27	of	of	ADP
eurjchem-1700	132	28	the	the	DET
eurjchem-1700	132	29	present	present	ADJ
eurjchem-1700	132	30	method	method	NOUN
eurjchem-1700	132	31	.	.	PUNCT
eurjchem-1700	133	1	the	the	DET
eurjchem-1700	133	2	correlation	correlation	NOUN
eurjchem-1700	133	3	coefficient	coefficient	NOUN
eurjchem-1700	133	4	(	(	PUNCT
eurjchem-1700	133	5	r2	r2	PROPN
eurjchem-1700	133	6	)	)	PUNCT
eurjchem-1700	133	7	was	be	AUX
eurjchem-1700	133	8	found	find	VERB
eurjchem-1700	133	9	to	to	PART
eurjchem-1700	133	10	be	be	AUX
eurjchem-1700	133	11	>	>	ADP
eurjchem-1700	133	12	0.999	0.999	NUM
eurjchem-1700	133	13	.	.	PUNCT
eurjchem-1700	134	1	the	the	DET
eurjchem-1700	134	2	linearity	linearity	NOUN
eurjchem-1700	134	3	results	result	NOUN
eurjchem-1700	134	4	are	be	AUX
eurjchem-1700	134	5	presented	present	VERB
eurjchem-1700	134	6	in	in	ADP
eurjchem-1700	134	7	table	table	NOUN
eurjchem-1700	134	8	1	1	NUM
eurjchem-1700	134	9	and	and	CCONJ
eurjchem-1700	134	10	the	the	DET
eurjchem-1700	134	11	standard	standard	ADJ
eurjchem-1700	134	12	deviation	deviation	NOUN
eurjchem-1700	134	13	(	(	PUNCT
eurjchem-1700	134	14	sd	sd	NOUN
eurjchem-1700	134	15	)	)	PUNCT
eurjchem-1700	134	16	and	and	CCONJ
eurjchem-1700	134	17	%	%	NOUN
eurjchem-1700	134	18	rsd	rsd	NOUN
eurjchem-1700	134	19	of	of	ADP
eurjchem-1700	134	20	the	the	DET
eurjchem-1700	134	21	peak	peak	NOUN
eurjchem-1700	134	22	area	area	NOUN
eurjchem-1700	134	23	at	at	ADP
eurjchem-1700	134	24	each	each	DET
eurjchem-1700	134	25	concentration	concentration	NOUN
eurjchem-1700	134	26	has	have	AUX
eurjchem-1700	134	27	been	be	AUX
eurjchem-1700	134	28	shown	show	VERB
eurjchem-1700	134	29	in	in	ADP
eurjchem-1700	134	30	table	table	NOUN
eurjchem-1700	134	31	2	2	NUM
eurjchem-1700	134	32	.	.	PUNCT
eurjchem-1700	135	1	the	the	DET
eurjchem-1700	135	2	method	method	PROPN
eurjchem-1700	135	3	precision	precision	NOUN
eurjchem-1700	135	4	experiment	experiment	NOUN
eurjchem-1700	135	5	was	be	AUX
eurjchem-1700	135	6	carried	carry	VERB
eurjchem-1700	135	7	out	out	ADP
eurjchem-1700	135	8	to	to	PART
eurjchem-1700	135	9	check	check	VERB
eurjchem-1700	135	10	the	the	DET
eurjchem-1700	135	11	variation	variation	NOUN
eurjchem-1700	135	12	among	among	ADP
eurjchem-1700	135	13	the	the	DET
eurjchem-1700	135	14	analysis	analysis	NOUN
eurjchem-1700	135	15	of	of	ADP
eurjchem-1700	135	16	multiple	multiple	ADJ
eurjchem-1700	135	17	sampling	sampling	NOUN
eurjchem-1700	135	18	of	of	ADP
eurjchem-1700	135	19	the	the	DET
eurjchem-1700	135	20	same	same	ADJ
eurjchem-1700	135	21	sample	sample	NOUN
eurjchem-1700	135	22	at	at	ADP
eurjchem-1700	135	23	laboratory	laboratory	NOUN
eurjchem-1700	135	24	condition	condition	NOUN
eurjchem-1700	135	25	.	.	PUNCT
eurjchem-1700	136	1	2018	2018	NUM
eurjchem-1700	136	2	–	–	PUNCT
eurjchem-1700	136	3	european	european	ADJ
eurjchem-1700	136	4	journal	journal	NOUN
eurjchem-1700	136	5	of	of	ADP
eurjchem-1700	136	6	chemistry	chemistry	NOUN
eurjchem-1700	136	7	–	–	PUNCT
eurjchem-1700	136	8	cc	cc	NOUN
eurjchem-1700	136	9	by	by	ADP
eurjchem-1700	136	10	nc	nc	PROPN
eurjchem-1700	136	11	–	–	PUNCT
eurjchem-1700	136	12	doi	doi	PROPN
eurjchem-1700	136	13	:	:	PUNCT
eurjchem-1700	136	14	10.5155	10.5155	NUM
eurjchem-1700	136	15	/	/	SYM
eurjchem-1700	136	16	eurjchem.9.2.92	eurjchem.9.2.92	NOUN
eurjchem-1700	136	17	-	-	PUNCT
eurjchem-1700	136	18	98.1700	98.1700	NUM
eurjchem-1700	136	19	96	96	NUM
eurjchem-1700	136	20	alhazmi	alhazmi	PROPN
eurjchem-1700	136	21	et	et	PROPN
eurjchem-1700	136	22	al	al	PROPN
eurjchem-1700	136	23	.	.	PUNCT
eurjchem-1700	136	24	/	/	SYM
eurjchem-1700	136	25	european	european	PROPN
eurjchem-1700	136	26	journal	journal	PROPN
eurjchem-1700	136	27	of	of	ADP
eurjchem-1700	136	28	chemistry	chemistry	NOUN
eurjchem-1700	136	29	9	9	NUM
eurjchem-1700	136	30	(	(	PUNCT
eurjchem-1700	136	31	2	2	NUM
eurjchem-1700	136	32	)	)	PUNCT
eurjchem-1700	136	33	(	(	PUNCT
eurjchem-1700	136	34	2018	2018	NUM
eurjchem-1700	136	35	)	)	PUNCT
eurjchem-1700	136	36	92	92	NUM
eurjchem-1700	136	37	-	-	SYM
eurjchem-1700	136	38	98	98	NUM
eurjchem-1700	136	39	table	table	NOUN
eurjchem-1700	136	40	3	3	NUM
eurjchem-1700	136	41	.	.	PUNCT
eurjchem-1700	136	42	intra	intra	ADJ
eurjchem-1700	136	43	-	-	NOUN
eurjchem-1700	136	44	day	day	NOUN
eurjchem-1700	136	45	and	and	CCONJ
eurjchem-1700	136	46	inter	inter	ADJ
eurjchem-1700	136	47	-	-	ADJ
eurjchem-1700	136	48	day	day	ADJ
eurjchem-1700	136	49	precision	precision	NOUN
eurjchem-1700	136	50	results	result	NOUN
eurjchem-1700	136	51	of	of	ADP
eurjchem-1700	136	52	clobetasone	clobetasone	NOUN
eurjchem-1700	136	53	butyrate	butyrate	NOUN
eurjchem-1700	136	54	cream	cream	NOUN
eurjchem-1700	136	55	(	(	PUNCT
eurjchem-1700	136	56	0.05	0.05	NUM
eurjchem-1700	136	57	%	%	NOUN
eurjchem-1700	136	58	,	,	PUNCT
eurjchem-1700	136	59	w	w	NOUN
eurjchem-1700	136	60	:	:	SYM
eurjchem-1700	136	61	w	w	X
eurjchem-1700	136	62	)	)	PUNCT
eurjchem-1700	136	63	by	by	ADP
eurjchem-1700	136	64	the	the	DET
eurjchem-1700	136	65	proposed	propose	VERB
eurjchem-1700	136	66	method	method	NOUN
eurjchem-1700	136	67	.	.	PUNCT
eurjchem-1700	137	1	experiment	experiment	NOUN
eurjchem-1700	137	2	assay	assay	NOUN
eurjchem-1700	137	3	%	%	NOUN
eurjchem-1700	137	4	average	average	ADJ
eurjchem-1700	137	5	%	%	NOUN
eurjchem-1700	137	6	assay	assay	PROPN
eurjchem-1700	137	7	±	±	NUM
eurjchem-1700	137	8	%	%	PROPN
eurjchem-1700	137	9	rsd	rsd	PROPN
eurjchem-1700	137	10	intra	intra	PROPN
eurjchem-1700	137	11	-	-	ADJ
eurjchem-1700	137	12	day	day	NOUN
eurjchem-1700	137	13	assay	assay	NOUN
eurjchem-1700	137	14	(	(	PUNCT
eurjchem-1700	137	15	n	n	NOUN
eurjchem-1700	137	16	=	=	SYM
eurjchem-1700	137	17	6	6	NUM
eurjchem-1700	137	18	)	)	PUNCT
eurjchem-1700	137	19	100.97	100.97	NUM
eurjchem-1700	137	20	100.19±0.94	100.19±0.94	NUM
eurjchem-1700	137	21	100.84	100.84	NUM
eurjchem-1700	137	22	99.11	99.11	NUM
eurjchem-1700	137	23	100.91	100.91	NUM
eurjchem-1700	137	24	100.43	100.43	NUM
eurjchem-1700	137	25	98.90	98.90	NUM
eurjchem-1700	137	26	inter	inter	ADJ
eurjchem-1700	137	27	-	-	ADJ
eurjchem-1700	137	28	day	day	NOUN
eurjchem-1700	137	29	assay	assay	NOUN
eurjchem-1700	137	30	(	(	PUNCT
eurjchem-1700	137	31	n	n	NOUN
eurjchem-1700	137	32	=	=	SYM
eurjchem-1700	137	33	6	6	NUM
eurjchem-1700	137	34	)	)	PUNCT
eurjchem-1700	137	35	100.17	100.17	NUM
eurjchem-1700	137	36	99.21±0.88	99.21±0.88	NUM
eurjchem-1700	137	37	100.30	100.30	NUM
eurjchem-1700	137	38	99.01	99.01	NUM
eurjchem-1700	137	39	98.67	98.67	NUM
eurjchem-1700	137	40	98.04	98.04	NUM
eurjchem-1700	137	41	99.06	99.06	NUM
eurjchem-1700	137	42	table	table	NOUN
eurjchem-1700	137	43	4	4	NUM
eurjchem-1700	137	44	.	.	PUNCT
eurjchem-1700	137	45	accuracy	accuracy	NOUN
eurjchem-1700	137	46	(	(	PUNCT
eurjchem-1700	137	47	recovery	recovery	NOUN
eurjchem-1700	137	48	)	)	PUNCT
eurjchem-1700	137	49	results	result	NOUN
eurjchem-1700	137	50	of	of	ADP
eurjchem-1700	137	51	clobetasone	clobetasone	NOUN
eurjchem-1700	137	52	butyrate	butyrate	NOUN
eurjchem-1700	137	53	cream	cream	NOUN
eurjchem-1700	137	54	.	.	PUNCT
eurjchem-1700	138	1	amount	amount	NOUN
eurjchem-1700	138	2	of	of	ADP
eurjchem-1700	138	3	drug	drug	NOUN
eurjchem-1700	138	4	present	present	ADJ
eurjchem-1700	138	5	in	in	ADP
eurjchem-1700	138	6	preanalysed	preanalysed	ADJ
eurjchem-1700	138	7	sample	sample	NOUN
eurjchem-1700	138	8	(	(	PUNCT
eurjchem-1700	138	9	µg	µg	NOUN
eurjchem-1700	138	10	/	/	SYM
eurjchem-1700	138	11	ml	ml	NOUN
eurjchem-1700	138	12	)	)	PUNCT
eurjchem-1700	138	13	amount	amount	NOUN
eurjchem-1700	138	14	of	of	ADP
eurjchem-1700	138	15	standard	standard	ADJ
eurjchem-1700	138	16	drug	drug	NOUN
eurjchem-1700	138	17	(	(	PUNCT
eurjchem-1700	138	18	rs	rs	NOUN
eurjchem-1700	138	19	)	)	PUNCT
eurjchem-1700	138	20	added	add	VERB
eurjchem-1700	138	21	(	(	PUNCT
eurjchem-1700	138	22	µg	µg	ADJ
eurjchem-1700	138	23	/	/	SYM
eurjchem-1700	138	24	ml	ml	NOUN
eurjchem-1700	138	25	)	)	PUNCT
eurjchem-1700	138	26	percentage	percentage	NOUN
eurjchem-1700	138	27	of	of	ADP
eurjchem-1700	138	28	concentration	concentration	NOUN
eurjchem-1700	138	29	level	level	NOUN
eurjchem-1700	138	30	added	add	VERB
eurjchem-1700	138	31	amount	amount	NOUN
eurjchem-1700	138	32	of	of	ADP
eurjchem-1700	138	33	drug	drug	NOUN
eurjchem-1700	138	34	recovered	recover	VERB
eurjchem-1700	138	35	(	(	PUNCT
eurjchem-1700	138	36	µg	µg	NOUN
eurjchem-1700	138	37	/	/	SYM
eurjchem-1700	138	38	ml	ml	NOUN
eurjchem-1700	138	39	)	)	PUNCT
eurjchem-1700	138	40	%	%	NOUN
eurjchem-1700	138	41	recovery	recovery	NOUN
eurjchem-1700	138	42	±	±	NUM
eurjchem-1700	138	43	sd	sd	NOUN
eurjchem-1700	138	44	;	;	PUNCT
eurjchem-1700	138	45	%	%	NOUN
eurjchem-1700	138	46	rsd	rsd	NOUN
eurjchem-1700	138	47	*	*	PUNCT
eurjchem-1700	138	48	25	25	NUM
eurjchem-1700	138	49	12.5	12.5	NUM
eurjchem-1700	138	50	50	50	NUM
eurjchem-1700	138	51	%	%	NOUN
eurjchem-1700	138	52	37.32	37.32	NUM
eurjchem-1700	138	53	99.51±1.46	99.51±1.46	NUM
eurjchem-1700	138	54	;	;	PUNCT
eurjchem-1700	138	55	1.47	1.47	NUM
eurjchem-1700	138	56	25	25	NUM
eurjchem-1700	138	57	25.0	25.0	NUM
eurjchem-1700	138	58	100	100	NUM
eurjchem-1700	138	59	%	%	NOUN
eurjchem-1700	138	60	49.58	49.58	NUM
eurjchem-1700	138	61	99.15±1.13	99.15±1.13	NUM
eurjchem-1700	138	62	;	;	PUNCT
eurjchem-1700	138	63	1.14	1.14	NUM
eurjchem-1700	138	64	25	25	NUM
eurjchem-1700	138	65	37.5	37.5	NUM
eurjchem-1700	138	66	150	150	NUM
eurjchem-1700	138	67	%	%	NOUN
eurjchem-1700	138	68	61.60	61.60	NUM
eurjchem-1700	138	69	98.56±0.68	98.56±0.68	NUM
eurjchem-1700	138	70	;	;	PUNCT
eurjchem-1700	138	71	0.69	0.69	NUM
eurjchem-1700	138	72	*	*	NOUN
eurjchem-1700	138	73	values	value	NOUN
eurjchem-1700	138	74	for	for	ADP
eurjchem-1700	138	75	three	three	NUM
eurjchem-1700	138	76	determinations	determination	NOUN
eurjchem-1700	138	77	.	.	PUNCT
eurjchem-1700	139	1	table	table	NOUN
eurjchem-1700	139	2	5	5	NUM
eurjchem-1700	139	3	.	.	PUNCT
eurjchem-1700	140	1	summary	summary	NOUN
eurjchem-1700	140	2	of	of	ADP
eurjchem-1700	140	3	force	force	NOUN
eurjchem-1700	140	4	degradation	degradation	NOUN
eurjchem-1700	140	5	results	result	NOUN
eurjchem-1700	140	6	of	of	ADP
eurjchem-1700	140	7	clobetasone	clobetasone	NOUN
eurjchem-1700	140	8	butyrate	butyrate	NOUN
eurjchem-1700	140	9	cream	cream	NOUN
eurjchem-1700	140	10	*	*	PUNCT
eurjchem-1700	140	11	.	.	PUNCT
eurjchem-1700	141	1	stress	stress	NOUN
eurjchem-1700	141	2	conditions	condition	NOUN
eurjchem-1700	141	3	peak	peak	VERB
eurjchem-1700	141	4	purity	purity	NOUN
eurjchem-1700	141	5	check	check	NOUN
eurjchem-1700	141	6	of	of	ADP
eurjchem-1700	141	7	the	the	DET
eurjchem-1700	141	8	main	main	ADJ
eurjchem-1700	141	9	peak	peak	NOUN
eurjchem-1700	141	10	average	average	ADJ
eurjchem-1700	141	11	%	%	NOUN
eurjchem-1700	141	12	assay	assay	PROPN
eurjchem-1700	141	13	±	±	PROPN
eurjchem-1700	141	14	sd	sd	ADP
eurjchem-1700	141	15	acid	acid	NOUN
eurjchem-1700	141	16	hydrolysis	hydrolysis	NOUN
eurjchem-1700	141	17	(	(	PUNCT
eurjchem-1700	141	18	4	4	NUM
eurjchem-1700	141	19	n	n	PRON
eurjchem-1700	141	20	hcl	hcl	PROPN
eurjchem-1700	141	21	,	,	PUNCT
eurjchem-1700	141	22	rt	rt	PROPN
eurjchem-1700	141	23	,	,	PUNCT
eurjchem-1700	141	24	60	60	NUM
eurjchem-1700	141	25	min	min	NOUN
eurjchem-1700	141	26	,	,	PUNCT
eurjchem-1700	141	27	n	n	NOUN
eurjchem-1700	141	28	=	=	SYM
eurjchem-1700	141	29	4	4	X
eurjchem-1700	141	30	)	)	PUNCT
eurjchem-1700	141	31	passed	pass	VERB
eurjchem-1700	141	32	99.022±0.772	99.022±0.772	NUM
eurjchem-1700	141	33	base	base	NOUN
eurjchem-1700	141	34	hydrolysis	hydrolysis	NOUN
eurjchem-1700	141	35	(	(	PUNCT
eurjchem-1700	141	36	1	1	NUM
eurjchem-1700	141	37	n	n	PRON
eurjchem-1700	141	38	naoh	naoh	NOUN
eurjchem-1700	141	39	,	,	PUNCT
eurjchem-1700	141	40	rt	rt	PROPN
eurjchem-1700	141	41	,	,	PUNCT
eurjchem-1700	141	42	6	6	NUM
eurjchem-1700	141	43	h	h	NOUN
eurjchem-1700	141	44	,	,	PUNCT
eurjchem-1700	141	45	n	n	NOUN
eurjchem-1700	141	46	=	=	SYM
eurjchem-1700	141	47	4	4	X
eurjchem-1700	141	48	)	)	PUNCT
eurjchem-1700	141	49	passed	pass	VERB
eurjchem-1700	141	50	99.213±0.843	99.213±0.843	NUM
eurjchem-1700	141	51	thermal	thermal	ADJ
eurjchem-1700	141	52	degradation	degradation	NOUN
eurjchem-1700	141	53	(	(	PUNCT
eurjchem-1700	141	54	on	on	ADP
eurjchem-1700	141	55	water	water	NOUN
eurjchem-1700	141	56	bath	bath	NOUN
eurjchem-1700	141	57	,	,	PUNCT
eurjchem-1700	141	58	~100	~100	NUM
eurjchem-1700	141	59	°	°	NOUN
eurjchem-1700	141	60	c	c	NOUN
eurjchem-1700	141	61	,	,	PUNCT
eurjchem-1700	141	62	6	6	NUM
eurjchem-1700	141	63	h	h	NOUN
eurjchem-1700	141	64	,	,	PUNCT
eurjchem-1700	141	65	n	n	NOUN
eurjchem-1700	141	66	=	=	SYM
eurjchem-1700	141	67	4	4	X
eurjchem-1700	141	68	)	)	PUNCT
eurjchem-1700	141	69	passed	pass	VERB
eurjchem-1700	141	70	82.117±1.113	82.117±1.113	NUM
eurjchem-1700	141	71	oxidative	oxidative	ADJ
eurjchem-1700	141	72	degradation	degradation	NOUN
eurjchem-1700	141	73	(	(	PUNCT
eurjchem-1700	141	74	30	30	NUM
eurjchem-1700	141	75	%	%	NOUN
eurjchem-1700	141	76	h2o2	h2o2	NOUN
eurjchem-1700	141	77	,	,	PUNCT
eurjchem-1700	141	78	rt	rt	NOUN
eurjchem-1700	141	79	,	,	PUNCT
eurjchem-1700	141	80	6	6	NUM
eurjchem-1700	141	81	h	h	NOUN
eurjchem-1700	141	82	,	,	PUNCT
eurjchem-1700	141	83	n	n	NOUN
eurjchem-1700	141	84	=	=	SYM
eurjchem-1700	141	85	4	4	X
eurjchem-1700	141	86	)	)	PUNCT
eurjchem-1700	141	87	passed	pass	VERB
eurjchem-1700	141	88	98.467±1.032	98.467±1.032	NUM
eurjchem-1700	141	89	photolytic	photolytic	ADJ
eurjchem-1700	141	90	degradation	degradation	NOUN
eurjchem-1700	141	91	(	(	PUNCT
eurjchem-1700	141	92	direct	direct	ADJ
eurjchem-1700	141	93	sunlight	sunlight	NOUN
eurjchem-1700	141	94	,	,	PUNCT
eurjchem-1700	141	95	6	6	NUM
eurjchem-1700	141	96	h	h	NOUN
eurjchem-1700	141	97	,	,	PUNCT
eurjchem-1700	141	98	n	n	NOUN
eurjchem-1700	141	99	=	=	SYM
eurjchem-1700	141	100	4	4	X
eurjchem-1700	141	101	)	)	PUNCT
eurjchem-1700	141	102	passed	pass	VERB
eurjchem-1700	141	103	78.764±1.213	78.764±1.213	NUM
eurjchem-1700	141	104	*	*	SYM
eurjchem-1700	141	105	sd	sd	NOUN
eurjchem-1700	141	106	is	be	AUX
eurjchem-1700	141	107	standard	standard	ADJ
eurjchem-1700	141	108	deviation	deviation	NOUN
eurjchem-1700	141	109	;	;	PUNCT
eurjchem-1700	141	110	rt	rt	NOUN
eurjchem-1700	141	111	=	=	PUNCT
eurjchem-1700	141	112	room	room	NOUN
eurjchem-1700	141	113	temperature	temperature	NOUN
eurjchem-1700	141	114	.	.	PUNCT
eurjchem-1700	142	1	the	the	DET
eurjchem-1700	142	2	intra	intra	ADJ
eurjchem-1700	142	3	-	-	ADJ
eurjchem-1700	142	4	day	day	ADJ
eurjchem-1700	142	5	method	method	NOUN
eurjchem-1700	142	6	precision	precision	NOUN
eurjchem-1700	142	7	was	be	AUX
eurjchem-1700	142	8	established	establish	VERB
eurjchem-1700	142	9	by	by	ADP
eurjchem-1700	142	10	performing	perform	VERB
eurjchem-1700	142	11	six	six	NUM
eurjchem-1700	142	12	independent	independent	ADJ
eurjchem-1700	142	13	assay	assay	NOUN
eurjchem-1700	142	14	analysis	analysis	NOUN
eurjchem-1700	142	15	of	of	ADP
eurjchem-1700	142	16	clobetasone	clobetasone	NOUN
eurjchem-1700	142	17	butyrate	butyrate	NOUN
eurjchem-1700	142	18	cream	cream	NOUN
eurjchem-1700	142	19	at	at	ADP
eurjchem-1700	142	20	different	different	ADJ
eurjchem-1700	142	21	times	time	NOUN
eurjchem-1700	142	22	of	of	ADP
eurjchem-1700	142	23	the	the	DET
eurjchem-1700	142	24	same	same	ADJ
eurjchem-1700	142	25	day	day	NOUN
eurjchem-1700	142	26	.	.	PUNCT
eurjchem-1700	143	1	whereas	whereas	SCONJ
eurjchem-1700	143	2	,	,	PUNCT
eurjchem-1700	143	3	the	the	DET
eurjchem-1700	143	4	reproducibility	reproducibility	NOUN
eurjchem-1700	143	5	(	(	PUNCT
eurjchem-1700	143	6	intermediate	intermediate	ADJ
eurjchem-1700	143	7	precision	precision	NOUN
eurjchem-1700	143	8	)	)	PUNCT
eurjchem-1700	143	9	was	be	AUX
eurjchem-1700	143	10	evaluated	evaluate	VERB
eurjchem-1700	143	11	by	by	ADP
eurjchem-1700	143	12	performing	perform	VERB
eurjchem-1700	143	13	the	the	DET
eurjchem-1700	143	14	assay	assay	ADJ
eurjchem-1700	143	15	experiments	experiment	NOUN
eurjchem-1700	143	16	by	by	ADP
eurjchem-1700	143	17	different	different	ADJ
eurjchem-1700	143	18	analyst	analyst	NOUN
eurjchem-1700	143	19	of	of	ADP
eurjchem-1700	143	20	the	the	DET
eurjchem-1700	143	21	same	same	ADJ
eurjchem-1700	143	22	laboratory	laboratory	NOUN
eurjchem-1700	143	23	at	at	ADP
eurjchem-1700	143	24	different	different	ADJ
eurjchem-1700	143	25	day	day	NOUN
eurjchem-1700	143	26	.	.	PUNCT
eurjchem-1700	144	1	the	the	DET
eurjchem-1700	144	2	average	average	ADJ
eurjchem-1700	144	3	%	%	NOUN
eurjchem-1700	144	4	assay	assay	NOUN
eurjchem-1700	144	5	was	be	AUX
eurjchem-1700	144	6	calculated	calculate	VERB
eurjchem-1700	144	7	to	to	PART
eurjchem-1700	144	8	be	be	AUX
eurjchem-1700	144	9	100.19	100.19	NUM
eurjchem-1700	144	10	and	and	CCONJ
eurjchem-1700	144	11	99.21	99.21	NUM
eurjchem-1700	144	12	%	%	NOUN
eurjchem-1700	144	13	for	for	ADP
eurjchem-1700	144	14	intra	intra	ADJ
eurjchem-1700	144	15	-	-	NOUN
eurjchem-1700	144	16	day	day	NOUN
eurjchem-1700	144	17	and	and	CCONJ
eurjchem-1700	144	18	interday	interday	NOUN
eurjchem-1700	144	19	analysis	analysis	NOUN
eurjchem-1700	144	20	,	,	PUNCT
eurjchem-1700	144	21	with	with	ADP
eurjchem-1700	144	22	%	%	NOUN
eurjchem-1700	144	23	rsd	rsd	NOUN
eurjchem-1700	144	24	less	less	ADJ
eurjchem-1700	144	25	than	than	ADP
eurjchem-1700	144	26	1	1	NUM
eurjchem-1700	144	27	.	.	PUNCT
eurjchem-1700	145	1	the	the	DET
eurjchem-1700	145	2	low	low	ADJ
eurjchem-1700	145	3	%	%	NOUN
eurjchem-1700	145	4	rsd	rsd	NOUN
eurjchem-1700	145	5	values	value	NOUN
eurjchem-1700	145	6	have	have	AUX
eurjchem-1700	145	7	indicated	indicate	VERB
eurjchem-1700	145	8	the	the	DET
eurjchem-1700	145	9	current	current	ADJ
eurjchem-1700	145	10	hplc	hplc	NOUN
eurjchem-1700	145	11	method	method	NOUN
eurjchem-1700	145	12	is	be	AUX
eurjchem-1700	145	13	precise	precise	ADJ
eurjchem-1700	145	14	.	.	PUNCT
eurjchem-1700	146	1	the	the	DET
eurjchem-1700	146	2	method	method	PROPN
eurjchem-1700	146	3	precision	precision	NOUN
eurjchem-1700	146	4	data	datum	NOUN
eurjchem-1700	146	5	has	have	AUX
eurjchem-1700	146	6	been	be	AUX
eurjchem-1700	146	7	given	give	VERB
eurjchem-1700	146	8	in	in	ADP
eurjchem-1700	146	9	table	table	NOUN
eurjchem-1700	146	10	3	3	NUM
eurjchem-1700	146	11	.	.	PUNCT
eurjchem-1700	147	1	the	the	DET
eurjchem-1700	147	2	accuracy	accuracy	NOUN
eurjchem-1700	147	3	of	of	ADP
eurjchem-1700	147	4	the	the	DET
eurjchem-1700	147	5	developed	develop	VERB
eurjchem-1700	147	6	method	method	NOUN
eurjchem-1700	147	7	was	be	AUX
eurjchem-1700	147	8	evaluated	evaluate	VERB
eurjchem-1700	147	9	by	by	ADP
eurjchem-1700	147	10	adding	add	VERB
eurjchem-1700	147	11	the	the	DET
eurjchem-1700	147	12	standard	standard	ADJ
eurjchem-1700	147	13	clobetasone	clobetasone	NOUN
eurjchem-1700	147	14	butyrate	butyrate	NOUN
eurjchem-1700	147	15	into	into	ADP
eurjchem-1700	147	16	the	the	DET
eurjchem-1700	147	17	preanalysed	preanalyse	VERB
eurjchem-1700	147	18	sample	sample	NOUN
eurjchem-1700	147	19	of	of	ADP
eurjchem-1700	147	20	cream	cream	NOUN
eurjchem-1700	147	21	formulation	formulation	NOUN
eurjchem-1700	147	22	at	at	ADP
eurjchem-1700	147	23	50	50	NUM
eurjchem-1700	147	24	,	,	PUNCT
eurjchem-1700	147	25	100	100	NUM
eurjchem-1700	147	26	and	and	CCONJ
eurjchem-1700	147	27	150	150	NUM
eurjchem-1700	147	28	%	%	NOUN
eurjchem-1700	147	29	levels	level	NOUN
eurjchem-1700	147	30	of	of	ADP
eurjchem-1700	147	31	the	the	DET
eurjchem-1700	147	32	target	target	NOUN
eurjchem-1700	147	33	concentration	concentration	NOUN
eurjchem-1700	147	34	(	(	PUNCT
eurjchem-1700	147	35	25	25	NUM
eurjchem-1700	147	36	μg	μg	NOUN
eurjchem-1700	147	37	/	/	SYM
eurjchem-1700	147	38	ml	ml	NOUN
eurjchem-1700	147	39	)	)	PUNCT
eurjchem-1700	147	40	.	.	PUNCT
eurjchem-1700	148	1	the	the	DET
eurjchem-1700	148	2	experiment	experiment	NOUN
eurjchem-1700	148	3	was	be	AUX
eurjchem-1700	148	4	conducted	conduct	VERB
eurjchem-1700	148	5	in	in	ADP
eurjchem-1700	148	6	triplicate	triplicate	NOUN
eurjchem-1700	148	7	and	and	CCONJ
eurjchem-1700	148	8	the	the	DET
eurjchem-1700	148	9	average	average	ADJ
eurjchem-1700	148	10	%	%	NOUN
eurjchem-1700	148	11	recovery	recovery	NOUN
eurjchem-1700	148	12	at	at	ADP
eurjchem-1700	148	13	each	each	DET
eurjchem-1700	148	14	level	level	NOUN
eurjchem-1700	148	15	was	be	AUX
eurjchem-1700	148	16	found	find	VERB
eurjchem-1700	148	17	to	to	PART
eurjchem-1700	148	18	be	be	AUX
eurjchem-1700	148	19	in	in	ADP
eurjchem-1700	148	20	the	the	DET
eurjchem-1700	148	21	acceptable	acceptable	ADJ
eurjchem-1700	148	22	limit	limit	NOUN
eurjchem-1700	148	23	(	(	PUNCT
eurjchem-1700	148	24	±2	±2	NOUN
eurjchem-1700	148	25	%	%	NOUN
eurjchem-1700	148	26	)	)	PUNCT
eurjchem-1700	148	27	.	.	PUNCT
eurjchem-1700	149	1	the	the	DET
eurjchem-1700	149	2	observed	observe	VERB
eurjchem-1700	149	3	recovery	recovery	NOUN
eurjchem-1700	149	4	results	result	NOUN
eurjchem-1700	149	5	have	have	AUX
eurjchem-1700	149	6	demonstrated	demonstrate	VERB
eurjchem-1700	149	7	the	the	DET
eurjchem-1700	149	8	accuracy	accuracy	NOUN
eurjchem-1700	149	9	of	of	ADP
eurjchem-1700	149	10	the	the	DET
eurjchem-1700	149	11	developed	develop	VERB
eurjchem-1700	149	12	hplc	hplc	NOUN
eurjchem-1700	149	13	method	method	NOUN
eurjchem-1700	149	14	.	.	PUNCT
eurjchem-1700	150	1	percent	percent	NOUN
eurjchem-1700	150	2	recovery	recovery	NOUN
eurjchem-1700	150	3	values	value	NOUN
eurjchem-1700	150	4	along	along	ADP
eurjchem-1700	150	5	with	with	ADP
eurjchem-1700	150	6	standard	standard	ADJ
eurjchem-1700	150	7	deviation	deviation	NOUN
eurjchem-1700	150	8	and	and	CCONJ
eurjchem-1700	150	9	%	%	NOUN
eurjchem-1700	150	10	relative	relative	ADJ
eurjchem-1700	150	11	standard	standard	ADJ
eurjchem-1700	150	12	deviation	deviation	NOUN
eurjchem-1700	150	13	has	have	AUX
eurjchem-1700	150	14	been	be	AUX
eurjchem-1700	150	15	depicted	depict	VERB
eurjchem-1700	150	16	in	in	ADP
eurjchem-1700	150	17	table	table	NOUN
eurjchem-1700	150	18	4	4	NUM
eurjchem-1700	150	19	.	.	PUNCT
eurjchem-1700	151	1	the	the	DET
eurjchem-1700	151	2	sensitivity	sensitivity	NOUN
eurjchem-1700	151	3	of	of	ADP
eurjchem-1700	151	4	the	the	DET
eurjchem-1700	151	5	developed	develop	VERB
eurjchem-1700	151	6	hplc	hplc	NOUN
eurjchem-1700	151	7	method	method	NOUN
eurjchem-1700	151	8	was	be	AUX
eurjchem-1700	151	9	proved	prove	VERB
eurjchem-1700	151	10	by	by	ADP
eurjchem-1700	151	11	low	low	ADJ
eurjchem-1700	151	12	lod	lod	PROPN
eurjchem-1700	151	13	and	and	CCONJ
eurjchem-1700	151	14	loq	loq	PROPN
eurjchem-1700	151	15	values	value	NOUN
eurjchem-1700	151	16	,	,	PUNCT
eurjchem-1700	151	17	determined	determine	VERB
eurjchem-1700	151	18	at	at	ADP
eurjchem-1700	151	19	s	s	PROPN
eurjchem-1700	151	20	/	/	SYM
eurjchem-1700	151	21	n	n	PROPN
eurjchem-1700	151	22	of	of	ADP
eurjchem-1700	151	23	3:1	3:1	NUM
eurjchem-1700	151	24	and	and	CCONJ
eurjchem-1700	151	25	10:1	10:1	NUM
eurjchem-1700	151	26	respectively	respectively	ADV
eurjchem-1700	151	27	.	.	PUNCT
eurjchem-1700	152	1	the	the	DET
eurjchem-1700	152	2	lod	lod	PROPN
eurjchem-1700	152	3	and	and	CCONJ
eurjchem-1700	152	4	loq	loq	PROPN
eurjchem-1700	152	5	values	value	NOUN
eurjchem-1700	152	6	of	of	ADP
eurjchem-1700	152	7	clobetasone	clobetasone	NOUN
eurjchem-1700	152	8	butyrate	butyrate	NOUN
eurjchem-1700	152	9	by	by	ADP
eurjchem-1700	152	10	the	the	DET
eurjchem-1700	152	11	present	present	ADJ
eurjchem-1700	152	12	study	study	NOUN
eurjchem-1700	152	13	were	be	AUX
eurjchem-1700	152	14	found	find	VERB
eurjchem-1700	152	15	to	to	PART
eurjchem-1700	152	16	be	be	AUX
eurjchem-1700	152	17	0.85	0.85	NUM
eurjchem-1700	152	18	and	and	CCONJ
eurjchem-1700	152	19	2.83	2.83	NUM
eurjchem-1700	152	20	μg	μg	NOUN
eurjchem-1700	152	21	/	/	SYM
eurjchem-1700	152	22	ml	ml	PROPN
eurjchem-1700	152	23	.	.	PUNCT
eurjchem-1700	153	1	the	the	DET
eurjchem-1700	153	2	sample	sample	NOUN
eurjchem-1700	153	3	and	and	CCONJ
eurjchem-1700	153	4	standard	standard	ADJ
eurjchem-1700	153	5	solutions	solution	NOUN
eurjchem-1700	153	6	were	be	AUX
eurjchem-1700	153	7	found	find	VERB
eurjchem-1700	153	8	to	to	PART
eurjchem-1700	153	9	be	be	AUX
eurjchem-1700	153	10	stable	stable	ADJ
eurjchem-1700	153	11	when	when	SCONJ
eurjchem-1700	153	12	stored	store	VERB
eurjchem-1700	153	13	at	at	ADP
eurjchem-1700	153	14	normal	normal	ADJ
eurjchem-1700	153	15	laboratory	laboratory	NOUN
eurjchem-1700	153	16	temperature	temperature	NOUN
eurjchem-1700	153	17	for	for	ADP
eurjchem-1700	153	18	at	at	ADV
eurjchem-1700	153	19	least	least	ADJ
eurjchem-1700	153	20	24	24	NUM
eurjchem-1700	153	21	h	h	NOUN
eurjchem-1700	153	22	(	(	PUNCT
eurjchem-1700	153	23	bench	bench	NOUN
eurjchem-1700	153	24	-	-	PUNCT
eurjchem-1700	153	25	top	top	NOUN
eurjchem-1700	153	26	stability	stability	NOUN
eurjchem-1700	153	27	)	)	PUNCT
eurjchem-1700	153	28	and	and	CCONJ
eurjchem-1700	153	29	in	in	ADP
eurjchem-1700	153	30	the	the	DET
eurjchem-1700	153	31	refrigerator	refrigerator	NOUN
eurjchem-1700	153	32	for	for	ADP
eurjchem-1700	153	33	48	48	NUM
eurjchem-1700	153	34	h.	h.	NOUN
eurjchem-1700	153	35	the	the	DET
eurjchem-1700	153	36	solutions	solution	NOUN
eurjchem-1700	153	37	were	be	AUX
eurjchem-1700	153	38	assayed	assayed	ADJ
eurjchem-1700	153	39	at	at	ADP
eurjchem-1700	153	40	12	12	NUM
eurjchem-1700	153	41	h	h	NOUN
eurjchem-1700	153	42	interval	interval	NOUN
eurjchem-1700	153	43	and	and	CCONJ
eurjchem-1700	153	44	the	the	DET
eurjchem-1700	153	45	%	%	NOUN
eurjchem-1700	153	46	rsd	rsd	NOUN
eurjchem-1700	153	47	of	of	ADP
eurjchem-1700	153	48	the	the	DET
eurjchem-1700	153	49	assay	assay	NOUN
eurjchem-1700	153	50	results	result	NOUN
eurjchem-1700	153	51	was	be	AUX
eurjchem-1700	153	52	calculated	calculate	VERB
eurjchem-1700	153	53	as	as	ADP
eurjchem-1700	153	54	0.73	0.73	NUM
eurjchem-1700	153	55	and	and	CCONJ
eurjchem-1700	153	56	0.89	0.89	NUM
eurjchem-1700	153	57	%	%	NOUN
eurjchem-1700	153	58	at	at	ADP
eurjchem-1700	153	59	laboratory	laboratory	NOUN
eurjchem-1700	153	60	temperature	temperature	NOUN
eurjchem-1700	153	61	and	and	CCONJ
eurjchem-1700	153	62	refrigerator	refrigerator	NOUN
eurjchem-1700	153	63	,	,	PUNCT
eurjchem-1700	153	64	respectively	respectively	ADV
eurjchem-1700	153	65	.	.	PUNCT
eurjchem-1700	154	1	the	the	DET
eurjchem-1700	154	2	solution	solution	NOUN
eurjchem-1700	154	3	stability	stability	NOUN
eurjchem-1700	154	4	results	result	NOUN
eurjchem-1700	154	5	have	have	AUX
eurjchem-1700	154	6	indicated	indicate	VERB
eurjchem-1700	154	7	that	that	SCONJ
eurjchem-1700	154	8	the	the	DET
eurjchem-1700	154	9	analysis	analysis	NOUN
eurjchem-1700	154	10	can	can	AUX
eurjchem-1700	154	11	be	be	AUX
eurjchem-1700	154	12	performed	perform	VERB
eurjchem-1700	154	13	for	for	ADP
eurjchem-1700	154	14	at	at	ADV
eurjchem-1700	154	15	least	least	ADV
eurjchem-1700	154	16	24	24	NUM
eurjchem-1700	154	17	h	h	NOUN
eurjchem-1700	154	18	at	at	ADP
eurjchem-1700	154	19	the	the	DET
eurjchem-1700	154	20	laboratory	laboratory	NOUN
eurjchem-1700	154	21	conditions	condition	NOUN
eurjchem-1700	154	22	using	use	VERB
eurjchem-1700	154	23	the	the	DET
eurjchem-1700	154	24	same	same	ADJ
eurjchem-1700	154	25	sample	sample	NOUN
eurjchem-1700	154	26	and	and	CCONJ
eurjchem-1700	154	27	standard	standard	ADJ
eurjchem-1700	154	28	solution	solution	NOUN
eurjchem-1700	154	29	without	without	ADP
eurjchem-1700	154	30	any	any	DET
eurjchem-1700	154	31	loss	loss	NOUN
eurjchem-1700	154	32	of	of	ADP
eurjchem-1700	154	33	the	the	DET
eurjchem-1700	154	34	active	active	ADJ
eurjchem-1700	154	35	drug	drug	NOUN
eurjchem-1700	154	36	component	component	NOUN
eurjchem-1700	154	37	.	.	PUNCT
eurjchem-1700	155	1	the	the	DET
eurjchem-1700	155	2	specificity	specificity	NOUN
eurjchem-1700	155	3	and	and	CCONJ
eurjchem-1700	155	4	stability	stability	NOUN
eurjchem-1700	155	5	-	-	PUNCT
eurjchem-1700	155	6	indicating	indicate	VERB
eurjchem-1700	155	7	property	property	NOUN
eurjchem-1700	155	8	of	of	ADP
eurjchem-1700	155	9	the	the	DET
eurjchem-1700	155	10	developed	develop	VERB
eurjchem-1700	155	11	method	method	NOUN
eurjchem-1700	155	12	was	be	AUX
eurjchem-1700	155	13	evaluated	evaluate	VERB
eurjchem-1700	155	14	by	by	ADP
eurjchem-1700	155	15	performing	perform	VERB
eurjchem-1700	155	16	forced	force	VERB
eurjchem-1700	155	17	degradation	degradation	NOUN
eurjchem-1700	155	18	study	study	NOUN
eurjchem-1700	155	19	of	of	ADP
eurjchem-1700	155	20	clobetasone	clobetasone	NOUN
eurjchem-1700	155	21	cream	cream	NOUN
eurjchem-1700	155	22	samples	sample	NOUN
eurjchem-1700	155	23	.	.	PUNCT
eurjchem-1700	156	1	the	the	DET
eurjchem-1700	156	2	specificity	specificity	NOUN
eurjchem-1700	156	3	of	of	ADP
eurjchem-1700	156	4	an	an	DET
eurjchem-1700	156	5	analytical	analytical	ADJ
eurjchem-1700	156	6	method	method	NOUN
eurjchem-1700	156	7	is	be	AUX
eurjchem-1700	156	8	the	the	DET
eurjchem-1700	156	9	ability	ability	NOUN
eurjchem-1700	156	10	of	of	ADP
eurjchem-1700	156	11	the	the	DET
eurjchem-1700	156	12	method	method	NOUN
eurjchem-1700	156	13	to	to	PART
eurjchem-1700	156	14	detect	detect	VERB
eurjchem-1700	156	15	the	the	DET
eurjchem-1700	156	16	analyte	analyte	NOUN
eurjchem-1700	156	17	in	in	ADP
eurjchem-1700	156	18	the	the	DET
eurjchem-1700	156	19	presence	presence	NOUN
eurjchem-1700	156	20	of	of	ADP
eurjchem-1700	156	21	potential	potential	ADJ
eurjchem-1700	156	22	impurities	impurity	NOUN
eurjchem-1700	156	23	and	and	CCONJ
eurjchem-1700	156	24	other	other	ADJ
eurjchem-1700	156	25	components	component	NOUN
eurjchem-1700	156	26	present	present	ADJ
eurjchem-1700	156	27	in	in	ADP
eurjchem-1700	156	28	the	the	DET
eurjchem-1700	156	29	analytical	analytical	ADJ
eurjchem-1700	156	30	solution	solution	NOUN
eurjchem-1700	156	31	.	.	PUNCT
eurjchem-1700	157	1	in	in	ADP
eurjchem-1700	157	2	this	this	DET
eurjchem-1700	157	3	study	study	NOUN
eurjchem-1700	157	4	,	,	PUNCT
eurjchem-1700	157	5	the	the	DET
eurjchem-1700	157	6	forced	force	VERB
eurjchem-1700	157	7	degradation	degradation	NOUN
eurjchem-1700	157	8	was	be	AUX
eurjchem-1700	157	9	performed	perform	VERB
eurjchem-1700	157	10	by	by	ADP
eurjchem-1700	157	11	exposure	exposure	NOUN
eurjchem-1700	157	12	of	of	ADP
eurjchem-1700	157	13	cream	cream	NOUN
eurjchem-1700	157	14	samples	sample	NOUN
eurjchem-1700	157	15	to	to	ADP
eurjchem-1700	157	16	various	various	ADJ
eurjchem-1700	157	17	stressed	stress	VERB
eurjchem-1700	157	18	conditions	condition	NOUN
eurjchem-1700	157	19	such	such	ADJ
eurjchem-1700	157	20	as	as	ADP
eurjchem-1700	157	21	acid	acid	ADJ
eurjchem-1700	157	22	and	and	CCONJ
eurjchem-1700	157	23	base	base	NOUN
eurjchem-1700	157	24	hydrolysis	hydrolysis	NOUN
eurjchem-1700	157	25	,	,	PUNCT
eurjchem-1700	157	26	thermal	thermal	ADJ
eurjchem-1700	157	27	degradation	degradation	NOUN
eurjchem-1700	157	28	(	(	PUNCT
eurjchem-1700	157	29	wet	wet	ADJ
eurjchem-1700	157	30	heat	heat	NOUN
eurjchem-1700	157	31	)	)	PUNCT
eurjchem-1700	157	32	,	,	PUNCT
eurjchem-1700	157	33	peroxide	peroxide	NOUN
eurjchem-1700	157	34	oxidation	oxidation	NOUN
eurjchem-1700	157	35	and	and	CCONJ
eurjchem-1700	157	36	photolytic	photolytic	ADJ
eurjchem-1700	157	37	degradation	degradation	NOUN
eurjchem-1700	157	38	.	.	PUNCT
eurjchem-1700	158	1	the	the	DET
eurjchem-1700	158	2	stressed	stress	VERB
eurjchem-1700	158	3	samples	sample	NOUN
eurjchem-1700	158	4	were	be	AUX
eurjchem-1700	158	5	analysed	analyse	VERB
eurjchem-1700	158	6	and	and	CCONJ
eurjchem-1700	158	7	assay	assay	NOUN
eurjchem-1700	158	8	results	result	NOUN
eurjchem-1700	158	9	were	be	AUX
eurjchem-1700	158	10	calculated	calculate	VERB
eurjchem-1700	158	11	from	from	ADP
eurjchem-1700	158	12	the	the	DET
eurjchem-1700	158	13	observed	observe	VERB
eurjchem-1700	158	14	peak	peak	NOUN
eurjchem-1700	158	15	area	area	NOUN
eurjchem-1700	158	16	of	of	ADP
eurjchem-1700	158	17	the	the	DET
eurjchem-1700	158	18	main	main	ADJ
eurjchem-1700	158	19	analyte	analyte	NOUN
eurjchem-1700	158	20	.	.	PUNCT
eurjchem-1700	159	1	the	the	DET
eurjchem-1700	159	2	forced	force	VERB
eurjchem-1700	159	3	degradation	degradation	NOUN
eurjchem-1700	159	4	results	result	NOUN
eurjchem-1700	159	5	suggested	suggest	VERB
eurjchem-1700	159	6	that	that	SCONJ
eurjchem-1700	159	7	clobetasone	clobetasone	NOUN
eurjchem-1700	159	8	butyrate	butyrate	NOUN
eurjchem-1700	159	9	in	in	ADP
eurjchem-1700	159	10	cream	cream	NOUN
eurjchem-1700	159	11	sample	sample	NOUN
eurjchem-1700	159	12	showed	show	VERB
eurjchem-1700	159	13	highest	high	ADJ
eurjchem-1700	159	14	sensitivity	sensitivity	NOUN
eurjchem-1700	159	15	towards	towards	ADP
eurjchem-1700	159	16	photolytic	photolytic	ADJ
eurjchem-1700	159	17	degradation	degradation	NOUN
eurjchem-1700	159	18	;	;	PUNCT
eurjchem-1700	159	19	the	the	DET
eurjchem-1700	159	20	sample	sample	NOUN
eurjchem-1700	159	21	has	have	AUX
eurjchem-1700	159	22	been	be	AUX
eurjchem-1700	159	23	exposed	expose	VERB
eurjchem-1700	159	24	to	to	ADP
eurjchem-1700	159	25	direct	direct	ADJ
eurjchem-1700	159	26	sunlight	sunlight	NOUN
eurjchem-1700	159	27	for	for	ADP
eurjchem-1700	159	28	6	6	NUM
eurjchem-1700	159	29	h.	h.	NOUN
eurjchem-1700	159	30	the	the	DET
eurjchem-1700	159	31	assay	assay	PROPN
eurjchem-1700	159	32	result	result	NOUN
eurjchem-1700	159	33	was	be	AUX
eurjchem-1700	159	34	calculated	calculate	VERB
eurjchem-1700	159	35	to	to	PART
eurjchem-1700	159	36	be	be	AUX
eurjchem-1700	159	37	78.76	78.76	NUM
eurjchem-1700	159	38	%	%	NOUN
eurjchem-1700	159	39	indicating	indicate	VERB
eurjchem-1700	159	40	that	that	SCONJ
eurjchem-1700	159	41	21.24	21.24	NUM
eurjchem-1700	159	42	%	%	NOUN
eurjchem-1700	159	43	drug	drug	NOUN
eurjchem-1700	159	44	was	be	AUX
eurjchem-1700	159	45	degraded	degrade	VERB
eurjchem-1700	159	46	.	.	PUNCT
eurjchem-1700	160	1	the	the	DET
eurjchem-1700	160	2	major	major	ADJ
eurjchem-1700	160	3	degradation	degradation	NOUN
eurjchem-1700	160	4	product	product	NOUN
eurjchem-1700	160	5	peak	peak	NOUN
eurjchem-1700	160	6	was	be	AUX
eurjchem-1700	160	7	observed	observe	VERB
eurjchem-1700	160	8	at	at	ADP
eurjchem-1700	160	9	9.0	9.0	NUM
eurjchem-1700	160	10	min	min	NOUN
eurjchem-1700	160	11	.	.	PROPN
eurjchem-1700	160	12	after	after	SCONJ
eurjchem-1700	160	13	photolytic	photolytic	ADJ
eurjchem-1700	160	14	degradation	degradation	NOUN
eurjchem-1700	160	15	the	the	DET
eurjchem-1700	160	16	test	test	NOUN
eurjchem-1700	160	17	drug	drug	NOUN
eurjchem-1700	160	18	was	be	AUX
eurjchem-1700	160	19	remarkably	remarkably	ADV
eurjchem-1700	160	20	degraded	degrade	VERB
eurjchem-1700	160	21	by	by	ADP
eurjchem-1700	160	22	thermal	thermal	ADJ
eurjchem-1700	160	23	degradation	degradation	NOUN
eurjchem-1700	160	24	and	and	CCONJ
eurjchem-1700	160	25	the	the	DET
eurjchem-1700	160	26	assay	assay	NOUN
eurjchem-1700	160	27	was	be	AUX
eurjchem-1700	160	28	calculated	calculate	VERB
eurjchem-1700	160	29	as	as	ADP
eurjchem-1700	160	30	82.12	82.12	NUM
eurjchem-1700	160	31	%	%	NOUN
eurjchem-1700	160	32	,	,	PUNCT
eurjchem-1700	160	33	indicating	indicate	VERB
eurjchem-1700	160	34	the	the	DET
eurjchem-1700	160	35	decomposition	decomposition	NOUN
eurjchem-1700	160	36	of	of	ADP
eurjchem-1700	160	37	17.88	17.88	NUM
eurjchem-1700	160	38	%	%	NOUN
eurjchem-1700	160	39	of	of	ADP
eurjchem-1700	160	40	clobetasone	clobetasone	NOUN
eurjchem-1700	160	41	butyrate	butyrate	NOUN
eurjchem-1700	160	42	.	.	PUNCT
eurjchem-1700	161	1	the	the	DET
eurjchem-1700	161	2	two	two	NUM
eurjchem-1700	161	3	degradation	degradation	NOUN
eurjchem-1700	161	4	products	product	NOUN
eurjchem-1700	161	5	were	be	AUX
eurjchem-1700	161	6	eluted	elute	VERB
eurjchem-1700	161	7	at	at	ADP
eurjchem-1700	161	8	1.5	1.5	NUM
eurjchem-1700	161	9	and	and	CCONJ
eurjchem-1700	161	10	9.9	9.9	NUM
eurjchem-1700	161	11	min	min	NOUN
eurjchem-1700	161	12	.	.	PUNCT
eurjchem-1700	162	1	the	the	DET
eurjchem-1700	162	2	test	test	NOUN
eurjchem-1700	162	3	drug	drug	NOUN
eurjchem-1700	162	4	has	have	AUX
eurjchem-1700	162	5	exhibited	exhibit	VERB
eurjchem-1700	162	6	no	no	DET
eurjchem-1700	162	7	degradation	degradation	NOUN
eurjchem-1700	162	8	against	against	ADP
eurjchem-1700	162	9	acidic	acidic	ADJ
eurjchem-1700	162	10	and	and	CCONJ
eurjchem-1700	162	11	basic	basic	ADJ
eurjchem-1700	162	12	hydrolysis	hydrolysis	NOUN
eurjchem-1700	162	13	,	,	PUNCT
eurjchem-1700	162	14	while	while	SCONJ
eurjchem-1700	162	15	insignificant	insignificant	ADJ
eurjchem-1700	162	16	decomposition	decomposition	NOUN
eurjchem-1700	162	17	was	be	AUX
eurjchem-1700	162	18	observed	observe	VERB
eurjchem-1700	162	19	when	when	SCONJ
eurjchem-1700	162	20	exposed	expose	VERB
eurjchem-1700	162	21	to	to	AUX
eurjchem-1700	162	22	oxidative	oxidative	ADJ
eurjchem-1700	162	23	degradation	degradation	NOUN
eurjchem-1700	162	24	by	by	ADP
eurjchem-1700	162	25	hydrogen	hydrogen	NOUN
eurjchem-1700	162	26	peroxide	peroxide	NOUN
eurjchem-1700	162	27	(	(	PUNCT
eurjchem-1700	162	28	1	1	NUM
eurjchem-1700	162	29	-	-	SYM
eurjchem-1700	162	30	2	2	NUM
eurjchem-1700	162	31	%	%	NOUN
eurjchem-1700	162	32	degradation	degradation	NOUN
eurjchem-1700	162	33	)	)	PUNCT
eurjchem-1700	162	34	.	.	PUNCT
eurjchem-1700	163	1	the	the	DET
eurjchem-1700	163	2	specificity	specificity	NOUN
eurjchem-1700	163	3	(	(	PUNCT
eurjchem-1700	163	4	selectivity	selectivity	NOUN
eurjchem-1700	163	5	)	)	PUNCT
eurjchem-1700	163	6	was	be	AUX
eurjchem-1700	163	7	also	also	ADV
eurjchem-1700	163	8	demonstrated	demonstrate	VERB
eurjchem-1700	163	9	by	by	ADP
eurjchem-1700	163	10	the	the	DET
eurjchem-1700	163	11	peak	peak	NOUN
eurjchem-1700	163	12	purity	purity	NOUN
eurjchem-1700	163	13	of	of	ADP
eurjchem-1700	163	14	the	the	DET
eurjchem-1700	163	15	analyte	analyte	NOUN
eurjchem-1700	163	16	peak	peak	NOUN
eurjchem-1700	163	17	.	.	PUNCT
eurjchem-1700	164	1	the	the	DET
eurjchem-1700	164	2	chromatograms	chromatogram	NOUN
eurjchem-1700	164	3	from	from	ADP
eurjchem-1700	164	4	the	the	DET
eurjchem-1700	164	5	sample	sample	NOUN
eurjchem-1700	164	6	and	and	CCONJ
eurjchem-1700	164	7	standard	standard	ADJ
eurjchem-1700	164	8	solutions	solution	NOUN
eurjchem-1700	164	9	were	be	AUX
eurjchem-1700	164	10	compared	compare	VERB
eurjchem-1700	164	11	with	with	ADP
eurjchem-1700	164	12	the	the	DET
eurjchem-1700	164	13	blank	blank	ADJ
eurjchem-1700	164	14	chromatograms	chromatogram	NOUN
eurjchem-1700	164	15	and	and	CCONJ
eurjchem-1700	164	16	no	no	DET
eurjchem-1700	164	17	interference	interference	NOUN
eurjchem-1700	164	18	was	be	AUX
eurjchem-1700	164	19	observed	observe	VERB
eurjchem-1700	164	20	at	at	ADP
eurjchem-1700	164	21	the	the	DET
eurjchem-1700	164	22	retention	retention	NOUN
eurjchem-1700	164	23	time	time	NOUN
eurjchem-1700	164	24	of	of	ADP
eurjchem-1700	164	25	the	the	DET
eurjchem-1700	164	26	test	test	NOUN
eurjchem-1700	164	27	drug	drug	NOUN
eurjchem-1700	164	28	,	,	PUNCT
eurjchem-1700	164	29	which	which	PRON
eurjchem-1700	164	30	has	have	AUX
eurjchem-1700	164	31	further	far	ADV
eurjchem-1700	164	32	proved	prove	VERB
eurjchem-1700	164	33	the	the	DET
eurjchem-1700	164	34	specificity	specificity	NOUN
eurjchem-1700	164	35	of	of	ADP
eurjchem-1700	164	36	the	the	DET
eurjchem-1700	164	37	method	method	NOUN
eurjchem-1700	164	38	.	.	PUNCT
eurjchem-1700	165	1	the	the	DET
eurjchem-1700	165	2	chromatograms	chromatogram	NOUN
eurjchem-1700	165	3	of	of	ADP
eurjchem-1700	165	4	forced	force	VERB
eurjchem-1700	165	5	degradation	degradation	NOUN
eurjchem-1700	165	6	study	study	NOUN
eurjchem-1700	165	7	were	be	AUX
eurjchem-1700	165	8	represented	represent	VERB
eurjchem-1700	165	9	in	in	ADP
eurjchem-1700	165	10	figures	figure	NOUN
eurjchem-1700	165	11	4	4	NUM
eurjchem-1700	165	12	and	and	CCONJ
eurjchem-1700	165	13	5	5	NUM
eurjchem-1700	165	14	and	and	CCONJ
eurjchem-1700	165	15	the	the	DET
eurjchem-1700	165	16	degradation	degradation	NOUN
eurjchem-1700	165	17	results	result	NOUN
eurjchem-1700	165	18	have	have	AUX
eurjchem-1700	165	19	been	be	AUX
eurjchem-1700	165	20	summarized	summarize	VERB
eurjchem-1700	165	21	in	in	ADP
eurjchem-1700	165	22	table	table	NOUN
eurjchem-1700	165	23	5	5	NUM
eurjchem-1700	165	24	.	.	NOUN
eurjchem-1700	166	1	4	4	NUM
eurjchem-1700	166	2	.	.	X
eurjchem-1700	166	3	conclusion	conclusion	VERB
eurjchem-1700	166	4	a	a	DET
eurjchem-1700	166	5	simple	simple	ADJ
eurjchem-1700	166	6	and	and	CCONJ
eurjchem-1700	166	7	specific	specific	ADJ
eurjchem-1700	166	8	reversed	reverse	VERB
eurjchem-1700	166	9	-	-	PUNCT
eurjchem-1700	166	10	phase	phase	NOUN
eurjchem-1700	166	11	hplc	hplc	NOUN
eurjchem-1700	166	12	method	method	NOUN
eurjchem-1700	166	13	for	for	ADP
eurjchem-1700	166	14	the	the	DET
eurjchem-1700	166	15	determination	determination	NOUN
eurjchem-1700	166	16	of	of	ADP
eurjchem-1700	166	17	clobetasone	clobetasone	NOUN
eurjchem-1700	166	18	butyrate	butyrate	NOUN
eurjchem-1700	166	19	in	in	ADP
eurjchem-1700	166	20	bulk	bulk	ADJ
eurjchem-1700	166	21	and	and	CCONJ
eurjchem-1700	166	22	cream	cream	NOUN
eurjchem-1700	166	23	dosage	dosage	NOUN
eurjchem-1700	166	24	forms	form	NOUN
eurjchem-1700	166	25	has	have	AUX
eurjchem-1700	166	26	been	be	AUX
eurjchem-1700	166	27	successfully	successfully	ADV
eurjchem-1700	166	28	developed	develop	VERB
eurjchem-1700	166	29	.	.	PUNCT
eurjchem-1700	167	1	the	the	DET
eurjchem-1700	167	2	retention	retention	NOUN
eurjchem-1700	167	3	time	time	NOUN
eurjchem-1700	167	4	of	of	ADP
eurjchem-1700	167	5	the	the	DET
eurjchem-1700	167	6	analyte	analyte	NOUN
eurjchem-1700	167	7	was	be	AUX
eurjchem-1700	167	8	short	short	ADJ
eurjchem-1700	167	9	(	(	PUNCT
eurjchem-1700	167	10	~4	~4	NOUN
eurjchem-1700	167	11	min	min	NOUN
eurjchem-1700	167	12	)	)	PUNCT
eurjchem-1700	167	13	,	,	PUNCT
eurjchem-1700	167	14	the	the	DET
eurjchem-1700	167	15	peak	peak	NOUN
eurjchem-1700	167	16	shape	shape	NOUN
eurjchem-1700	167	17	was	be	AUX
eurjchem-1700	167	18	excellent	excellent	ADJ
eurjchem-1700	167	19	and	and	CCONJ
eurjchem-1700	167	20	the	the	DET
eurjchem-1700	167	21	system	system	NOUN
eurjchem-1700	167	22	suitability	suitability	NOUN
eurjchem-1700	167	23	parameters	parameter	NOUN
eurjchem-1700	167	24	were	be	AUX
eurjchem-1700	167	25	acceptable	acceptable	ADJ
eurjchem-1700	167	26	.	.	PUNCT
eurjchem-1700	168	1	the	the	DET
eurjchem-1700	168	2	method	method	NOUN
eurjchem-1700	168	3	was	be	AUX
eurjchem-1700	168	4	evaluated	evaluate	VERB
eurjchem-1700	168	5	according	accord	VERB
eurjchem-1700	168	6	to	to	ADP
eurjchem-1700	168	7	ich	ich	PROPN
eurjchem-1700	168	8	guidelines	guideline	NOUN
eurjchem-1700	168	9	q2	q2	NOUN
eurjchem-1700	168	10	r1	r1	PROPN
eurjchem-1700	168	11	and	and	CCONJ
eurjchem-1700	168	12	proved	prove	VERB
eurjchem-1700	168	13	to	to	PART
eurjchem-1700	168	14	be	be	AUX
eurjchem-1700	168	15	sensitive	sensitive	ADJ
eurjchem-1700	168	16	,	,	PUNCT
eurjchem-1700	168	17	linear	linear	ADJ
eurjchem-1700	168	18	,	,	PUNCT
eurjchem-1700	168	19	precise	precise	ADJ
eurjchem-1700	168	20	and	and	CCONJ
eurjchem-1700	168	21	accurate	accurate	ADJ
eurjchem-1700	168	22	for	for	ADP
eurjchem-1700	168	23	detection	detection	NOUN
eurjchem-1700	168	24	and	and	CCONJ
eurjchem-1700	168	25	estimation	estimation	NOUN
eurjchem-1700	168	26	of	of	ADP
eurjchem-1700	168	27	clobetasone	clobetasone	NOUN
eurjchem-1700	168	28	butyrate	butyrate	NOUN
eurjchem-1700	168	29	.	.	PUNCT
eurjchem-1700	169	1	the	the	DET
eurjchem-1700	169	2	method	method	NOUN
eurjchem-1700	169	3	has	have	AUX
eurjchem-1700	169	4	been	be	AUX
eurjchem-1700	169	5	subjected	subject	VERB
eurjchem-1700	169	6	to	to	ADP
eurjchem-1700	169	7	forced	force	VERB
eurjchem-1700	169	8	degradation	degradation	NOUN
eurjchem-1700	169	9	study	study	NOUN
eurjchem-1700	169	10	,	,	PUNCT
eurjchem-1700	169	11	which	which	PRON
eurjchem-1700	169	12	has	have	AUX
eurjchem-1700	169	13	demonstrated	demonstrate	VERB
eurjchem-1700	169	14	the	the	DET
eurjchem-1700	169	15	specificity	specificity	NOUN
eurjchem-1700	169	16	for	for	ADP
eurjchem-1700	169	17	the	the	DET
eurjchem-1700	169	18	analyte	analyte	NOUN
eurjchem-1700	169	19	.	.	PUNCT
eurjchem-1700	170	1	2018	2018	NUM
eurjchem-1700	170	2	–	–	PUNCT
eurjchem-1700	170	3	european	european	ADJ
eurjchem-1700	170	4	journal	journal	NOUN
eurjchem-1700	170	5	of	of	ADP
eurjchem-1700	170	6	chemistry	chemistry	NOUN
eurjchem-1700	170	7	–	–	PUNCT
eurjchem-1700	170	8	cc	cc	NOUN
eurjchem-1700	170	9	by	by	ADP
eurjchem-1700	170	10	nc	nc	PROPN
eurjchem-1700	170	11	–	–	PUNCT
eurjchem-1700	170	12	doi	doi	PROPN
eurjchem-1700	170	13	:	:	PUNCT
eurjchem-1700	170	14	10.5155	10.5155	NUM
eurjchem-1700	170	15	/	/	SYM
eurjchem-1700	170	16	eurjchem.9.2.92	eurjchem.9.2.92	NOUN
eurjchem-1700	170	17	-	-	SYM
eurjchem-1700	170	18	98.1700	98.1700	NUM
eurjchem-1700	170	19	alhazmi	alhazmi	NOUN
eurjchem-1700	170	20	et	et	NOUN
eurjchem-1700	170	21	al	al	PROPN
eurjchem-1700	170	22	.	.	PUNCT
eurjchem-1700	170	23	/	/	SYM
eurjchem-1700	170	24	european	european	PROPN
eurjchem-1700	170	25	journal	journal	PROPN
eurjchem-1700	170	26	of	of	ADP
eurjchem-1700	170	27	chemistry	chemistry	NOUN
eurjchem-1700	170	28	9	9	NUM
eurjchem-1700	170	29	(	(	PUNCT
eurjchem-1700	170	30	2	2	NUM
eurjchem-1700	170	31	)	)	PUNCT
eurjchem-1700	170	32	(	(	PUNCT
eurjchem-1700	170	33	2018	2018	NUM
eurjchem-1700	170	34	)	)	PUNCT
eurjchem-1700	170	35	92	92	NUM
eurjchem-1700	170	36	-	-	SYM
eurjchem-1700	170	37	98	98	NUM
eurjchem-1700	170	38	97	97	NUM
eurjchem-1700	170	39	(	(	PUNCT
eurjchem-1700	170	40	a	a	NOUN
eurjchem-1700	170	41	)	)	PUNCT
eurjchem-1700	170	42	(	(	PUNCT
eurjchem-1700	170	43	b	b	X
eurjchem-1700	170	44	)	)	PUNCT
eurjchem-1700	170	45	figure	figure	NOUN
eurjchem-1700	170	46	4	4	NUM
eurjchem-1700	170	47	.	.	PUNCT
eurjchem-1700	170	48	representative	representative	ADJ
eurjchem-1700	170	49	chromatograms	chromatogram	NOUN
eurjchem-1700	170	50	of	of	ADP
eurjchem-1700	170	51	forced	force	VERB
eurjchem-1700	170	52	degradation	degradation	NOUN
eurjchem-1700	170	53	samples	sample	NOUN
eurjchem-1700	170	54	:	:	PUNCT
eurjchem-1700	170	55	(	(	PUNCT
eurjchem-1700	170	56	a	a	X
eurjchem-1700	170	57	)	)	PUNCT
eurjchem-1700	170	58	acid	acid	NOUN
eurjchem-1700	170	59	degradation	degradation	NOUN
eurjchem-1700	170	60	and	and	CCONJ
eurjchem-1700	170	61	(	(	PUNCT
eurjchem-1700	170	62	b	b	NOUN
eurjchem-1700	170	63	)	)	PUNCT
eurjchem-1700	170	64	alkali	alkali	ADJ
eurjchem-1700	170	65	degradation	degradation	NOUN
eurjchem-1700	170	66	.	.	PUNCT
eurjchem-1700	171	1	(	(	PUNCT
eurjchem-1700	171	2	a	a	X
eurjchem-1700	171	3	)	)	PUNCT
eurjchem-1700	171	4	(	(	PUNCT
eurjchem-1700	171	5	b	b	X
eurjchem-1700	171	6	)	)	PUNCT
eurjchem-1700	171	7	(	(	PUNCT
eurjchem-1700	171	8	c	c	X
eurjchem-1700	171	9	)	)	PUNCT
eurjchem-1700	171	10	figure	figure	NOUN
eurjchem-1700	171	11	5	5	NUM
eurjchem-1700	171	12	.	.	PUNCT
eurjchem-1700	171	13	representative	representative	ADJ
eurjchem-1700	171	14	chromatograms	chromatogram	NOUN
eurjchem-1700	171	15	of	of	ADP
eurjchem-1700	171	16	forced	force	VERB
eurjchem-1700	171	17	degradation	degradation	NOUN
eurjchem-1700	171	18	samples	sample	NOUN
eurjchem-1700	171	19	:	:	PUNCT
eurjchem-1700	171	20	(	(	PUNCT
eurjchem-1700	171	21	a	a	X
eurjchem-1700	171	22	)	)	PUNCT
eurjchem-1700	171	23	wet	wet	ADJ
eurjchem-1700	171	24	heat	heat	NOUN
eurjchem-1700	171	25	degradation	degradation	NOUN
eurjchem-1700	171	26	;	;	PUNCT
eurjchem-1700	171	27	(	(	PUNCT
eurjchem-1700	171	28	b	b	X
eurjchem-1700	171	29	)	)	PUNCT
eurjchem-1700	171	30	photolytic	photolytic	ADJ
eurjchem-1700	171	31	degradation	degradation	NOUN
eurjchem-1700	171	32	and	and	CCONJ
eurjchem-1700	171	33	(	(	PUNCT
eurjchem-1700	171	34	c	c	NOUN
eurjchem-1700	171	35	)	)	PUNCT
eurjchem-1700	171	36	oxidative	oxidative	ADJ
eurjchem-1700	171	37	degradation	degradation	NOUN
eurjchem-1700	171	38	.	.	PUNCT
eurjchem-1700	172	1	2018	2018	NUM
eurjchem-1700	172	2	–	–	PUNCT
eurjchem-1700	172	3	european	european	ADJ
eurjchem-1700	172	4	journal	journal	NOUN
eurjchem-1700	172	5	of	of	ADP
eurjchem-1700	172	6	chemistry	chemistry	NOUN
eurjchem-1700	172	7	–	–	PUNCT
eurjchem-1700	172	8	cc	cc	NOUN
eurjchem-1700	172	9	by	by	ADP
eurjchem-1700	172	10	nc	nc	PROPN
eurjchem-1700	172	11	–	–	PUNCT
eurjchem-1700	172	12	doi	doi	PROPN
eurjchem-1700	172	13	:	:	PUNCT
eurjchem-1700	172	14	10.5155	10.5155	NUM
eurjchem-1700	172	15	/	/	SYM
eurjchem-1700	172	16	eurjchem.9.2.92	eurjchem.9.2.92	NOUN
eurjchem-1700	172	17	-	-	PUNCT
eurjchem-1700	172	18	98.1700	98.1700	NUM
eurjchem-1700	172	19	98	98	NUM
eurjchem-1700	172	20	alhazmi	alhazmi	NOUN
eurjchem-1700	172	21	et	et	NOUN
eurjchem-1700	172	22	al	al	PROPN
eurjchem-1700	172	23	.	.	PUNCT
eurjchem-1700	172	24	/	/	SYM
eurjchem-1700	172	25	european	european	PROPN
eurjchem-1700	172	26	journal	journal	PROPN
eurjchem-1700	172	27	of	of	ADP
eurjchem-1700	172	28	chemistry	chemistry	NOUN
eurjchem-1700	172	29	9	9	NUM
eurjchem-1700	172	30	(	(	PUNCT
eurjchem-1700	172	31	2	2	NUM
eurjchem-1700	172	32	)	)	PUNCT
eurjchem-1700	172	33	(	(	PUNCT
eurjchem-1700	172	34	2018	2018	NUM
eurjchem-1700	172	35	)	)	PUNCT
eurjchem-1700	172	36	92	92	NUM
eurjchem-1700	172	37	-	-	SYM
eurjchem-1700	172	38	98	98	NUM
eurjchem-1700	172	39	the	the	DET
eurjchem-1700	172	40	specificity	specificity	NOUN
eurjchem-1700	172	41	was	be	AUX
eurjchem-1700	172	42	further	far	ADV
eurjchem-1700	172	43	proved	prove	VERB
eurjchem-1700	172	44	by	by	ADP
eurjchem-1700	172	45	the	the	DET
eurjchem-1700	172	46	absence	absence	NOUN
eurjchem-1700	172	47	of	of	ADP
eurjchem-1700	172	48	any	any	DET
eurjchem-1700	172	49	interference	interference	NOUN
eurjchem-1700	172	50	from	from	ADP
eurjchem-1700	172	51	blank	blank	ADJ
eurjchem-1700	172	52	and	and	CCONJ
eurjchem-1700	172	53	placebo	placebo	NOUN
eurjchem-1700	172	54	at	at	ADP
eurjchem-1700	172	55	the	the	DET
eurjchem-1700	172	56	retention	retention	NOUN
eurjchem-1700	172	57	time	time	NOUN
eurjchem-1700	172	58	of	of	ADP
eurjchem-1700	172	59	the	the	DET
eurjchem-1700	172	60	analyte	analyte	NOUN
eurjchem-1700	172	61	.	.	PUNCT
eurjchem-1700	173	1	the	the	DET
eurjchem-1700	173	2	test	test	NOUN
eurjchem-1700	173	3	drug	drug	NOUN
eurjchem-1700	173	4	was	be	AUX
eurjchem-1700	173	5	found	find	VERB
eurjchem-1700	173	6	to	to	PART
eurjchem-1700	173	7	be	be	AUX
eurjchem-1700	173	8	stable	stable	ADJ
eurjchem-1700	173	9	in	in	ADP
eurjchem-1700	173	10	the	the	DET
eurjchem-1700	173	11	analytical	analytical	ADJ
eurjchem-1700	173	12	solutions	solution	NOUN
eurjchem-1700	173	13	for	for	ADP
eurjchem-1700	173	14	at	at	ADV
eurjchem-1700	173	15	least	least	ADV
eurjchem-1700	173	16	24	24	NUM
eurjchem-1700	173	17	h.	h.	NOUN
eurjchem-1700	173	18	the	the	DET
eurjchem-1700	173	19	current	current	ADJ
eurjchem-1700	173	20	method	method	NOUN
eurjchem-1700	173	21	can	can	AUX
eurjchem-1700	173	22	be	be	AUX
eurjchem-1700	173	23	used	use	VERB
eurjchem-1700	173	24	for	for	ADP
eurjchem-1700	173	25	stability	stability	NOUN
eurjchem-1700	173	26	indicating	indicate	VERB
eurjchem-1700	173	27	quantification	quantification	NOUN
eurjchem-1700	173	28	of	of	ADP
eurjchem-1700	173	29	the	the	DET
eurjchem-1700	173	30	test	test	NOUN
eurjchem-1700	173	31	drug	drug	NOUN
eurjchem-1700	173	32	in	in	ADP
eurjchem-1700	173	33	routine	routine	ADJ
eurjchem-1700	173	34	analysis	analysis	NOUN
eurjchem-1700	173	35	and	and	CCONJ
eurjchem-1700	173	36	quality	quality	NOUN
eurjchem-1700	173	37	control	control	NOUN
eurjchem-1700	173	38	of	of	ADP
eurjchem-1700	173	39	pharmaceutical	pharmaceutical	NOUN
eurjchem-1700	173	40	products	product	NOUN
eurjchem-1700	173	41	.	.	PUNCT
eurjchem-1700	174	1	disclosure	disclosure	NOUN
eurjchem-1700	174	2	statement	statement	NOUN
eurjchem-1700	174	3	conflict	conflict	NOUN
eurjchem-1700	174	4	of	of	ADP
eurjchem-1700	174	5	interests	interest	NOUN
eurjchem-1700	174	6	:	:	PUNCT
eurjchem-1700	174	7	the	the	DET
eurjchem-1700	174	8	authors	author	NOUN
eurjchem-1700	174	9	declare	declare	VERB
eurjchem-1700	174	10	that	that	SCONJ
eurjchem-1700	174	11	they	they	PRON
eurjchem-1700	174	12	have	have	VERB
eurjchem-1700	174	13	no	no	DET
eurjchem-1700	174	14	conflict	conflict	NOUN
eurjchem-1700	174	15	of	of	ADP
eurjchem-1700	174	16	interest	interest	NOUN
eurjchem-1700	174	17	.	.	PUNCT
eurjchem-1700	175	1	author	author	NOUN
eurjchem-1700	175	2	contributions	contribution	NOUN
eurjchem-1700	175	3	:	:	PUNCT
eurjchem-1700	175	4	all	all	DET
eurjchem-1700	175	5	authors	author	NOUN
eurjchem-1700	175	6	contributed	contribute	VERB
eurjchem-1700	175	7	equally	equally	ADV
eurjchem-1700	175	8	to	to	ADP
eurjchem-1700	175	9	this	this	DET
eurjchem-1700	175	10	work	work	NOUN
eurjchem-1700	175	11	.	.	PUNCT
eurjchem-1700	176	1	ethical	ethical	ADJ
eurjchem-1700	176	2	approval	approval	NOUN
eurjchem-1700	176	3	:	:	PUNCT
eurjchem-1700	177	1	all	all	DET
eurjchem-1700	177	2	ethical	ethical	ADJ
eurjchem-1700	177	3	guidelines	guideline	NOUN
eurjchem-1700	177	4	have	have	AUX
eurjchem-1700	177	5	been	be	AUX
eurjchem-1700	177	6	adhered	adhere	VERB
eurjchem-1700	177	7	.	.	PUNCT
eurjchem-1700	178	1	orcid	orcid	PROPN
eurjchem-1700	178	2	hassan	hassan	PROPN
eurjchem-1700	178	3	ahmad	ahmad	PROPN
eurjchem-1700	178	4	alhazmi	alhazmi	PROPN
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eurjchem-1700	178	6	gunasekar	gunasekar	PROPN
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eurjchem-1700	178	9	mohammed	mohammed	PROPN
eurjchem-1700	178	10	al	al	PROPN
eurjchem-1700	178	11	bratty	bratty	PROPN
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eurjchem-1700	178	13	sadique	sadique	ADJ
eurjchem-1700	178	14	akhtar	akhtar	PROPN
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eurjchem-1700	178	17	references	reference	NOUN
eurjchem-1700	178	18	[	[	X
eurjchem-1700	178	19	1	1	NUM
eurjchem-1700	178	20	]	]	PUNCT
eurjchem-1700	178	21	.	.	PUNCT
eurjchem-1700	179	1	munro	munro	PROPN
eurjchem-1700	179	2	,	,	PUNCT
eurjchem-1700	179	3	d.	d.	PROPN
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eurjchem-1700	179	5	;	;	PUNCT
eurjchem-1700	179	6	wilson	wilson	PROPN
eurjchem-1700	179	7	,	,	PUNCT
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eurjchem-1700	179	9	br	br	PROPN
eurjchem-1700	179	10	.	.	PUNCT
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eurjchem-1700	180	1	j.	j.	PROPN
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eurjchem-1700	180	3	,	,	PUNCT
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eurjchem-1700	180	5	,	,	PUNCT
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eurjchem-1700	181	1	[	[	X
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eurjchem-1700	181	3	]	]	PUNCT
eurjchem-1700	181	4	.	.	PUNCT
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eurjchem-1700	182	5	;	;	PUNCT
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eurjchem-1700	182	7	,	,	PUNCT
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eurjchem-1700	182	10	;	;	PUNCT
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eurjchem-1700	182	12	,	,	PUNCT
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eurjchem-1700	182	16	.	.	PUNCT
eurjchem-1700	183	1	j.	j.	PROPN
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eurjchem-1700	183	3	.	.	PUNCT
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eurjchem-1700	184	2	,	,	PUNCT
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eurjchem-1700	184	4	,	,	PUNCT
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eurjchem-1700	184	8	.	.	PUNCT
eurjchem-1700	185	1	[	[	X
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eurjchem-1700	185	3	]	]	PUNCT
eurjchem-1700	185	4	.	.	PUNCT
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eurjchem-1700	186	3	.	.	PUNCT
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eurjchem-1700	188	16	.	.	PUNCT
eurjchem-1700	189	1	[	[	X
eurjchem-1700	189	2	4	4	NUM
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eurjchem-1700	189	4	.	.	PUNCT
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eurjchem-1700	190	7	d.	d.	PROPN
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eurjchem-1700	190	9	;	;	PUNCT
eurjchem-1700	190	10	manna	manna	PROPN
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eurjchem-1700	191	2	.	.	PUNCT
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eurjchem-1700	192	2	.	.	PUNCT
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eurjchem-1700	193	2	.	.	PROPN
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eurjchem-1700	193	4	,	,	PUNCT
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eurjchem-1700	193	8	-	-	SYM
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eurjchem-1700	193	10	.	.	PUNCT
eurjchem-1700	194	1	[	[	X
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eurjchem-1700	194	3	]	]	PUNCT
eurjchem-1700	194	4	.	.	PUNCT
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eurjchem-1700	194	8	;	;	PUNCT
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eurjchem-1700	194	19	.	.	PUNCT
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eurjchem-1700	195	2	.	.	PUNCT
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eurjchem-1700	196	2	,	,	PUNCT
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eurjchem-1700	197	4	.	.	PUNCT
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eurjchem-1700	198	2	-	-	PUNCT
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eurjchem-1700	198	4	,	,	PUNCT
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eurjchem-1700	198	8	,	,	PUNCT
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eurjchem-1700	198	10	;	;	PUNCT
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eurjchem-1700	198	16	.	.	PUNCT
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eurjchem-1700	199	2	.	.	PUNCT
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eurjchem-1700	200	2	,	,	PUNCT
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eurjchem-1700	200	4	,	,	PUNCT
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eurjchem-1700	200	6	-	-	SYM
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eurjchem-1700	200	8	.	.	PUNCT
eurjchem-1700	201	1	[	[	X
eurjchem-1700	201	2	7	7	NUM
eurjchem-1700	201	3	]	]	PUNCT
eurjchem-1700	201	4	.	.	PUNCT
eurjchem-1700	202	1	williamson	williamson	PROPN
eurjchem-1700	202	2	,	,	PUNCT
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eurjchem-1700	202	4	;	;	PUNCT
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eurjchem-1700	202	6	,	,	PUNCT
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eurjchem-1700	202	9	;	;	PUNCT
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eurjchem-1700	202	11	,	,	PUNCT
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eurjchem-1700	202	15	.	.	PUNCT
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eurjchem-1700	204	2	.	.	PUNCT
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eurjchem-1700	205	2	.	.	PROPN
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eurjchem-1700	205	6	,	,	PUNCT
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eurjchem-1700	205	8	-	-	SYM
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eurjchem-1700	205	10	.	.	PUNCT
eurjchem-1700	206	1	[	[	X
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eurjchem-1700	206	4	.	.	PUNCT
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eurjchem-1700	207	5	;	;	PUNCT
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eurjchem-1700	207	17	.	.	PUNCT
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eurjchem-1700	210	2	,	,	PUNCT
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eurjchem-1700	210	4	,	,	PUNCT
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eurjchem-1700	210	8	.	.	PUNCT
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eurjchem-1700	211	4	.	.	PUNCT
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eurjchem-1700	212	23	.	.	PUNCT
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eurjchem-1700	213	4	,	,	PUNCT
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eurjchem-1700	213	6	,	,	PUNCT
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eurjchem-1700	213	8	-	-	SYM
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eurjchem-1700	213	10	.	.	PUNCT
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eurjchem-1700	214	3	]	]	PUNCT
eurjchem-1700	214	4	.	.	PUNCT
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eurjchem-1700	215	2	,	,	PUNCT
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eurjchem-1700	215	4	c.	c.	PROPN
eurjchem-1700	215	5	;	;	PUNCT
eurjchem-1700	215	6	bastos	basto	NOUN
eurjchem-1700	215	7	,	,	PUNCT
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eurjchem-1700	215	9	o.	o.	PROPN
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eurjchem-1700	215	18	.	.	PUNCT
eurjchem-1700	216	1	sci	sci	PROPN
eurjchem-1700	216	2	.	.	PROPN
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eurjchem-1700	216	4	,	,	PUNCT
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eurjchem-1700	216	6	,	,	PUNCT
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eurjchem-1700	216	8	-	-	SYM
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eurjchem-1700	216	10	.	.	PUNCT
eurjchem-1700	217	1	[	[	X
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eurjchem-1700	217	3	]	]	PUNCT
eurjchem-1700	217	4	.	.	PUNCT
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eurjchem-1700	218	2	,	,	PUNCT
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eurjchem-1700	218	5	;	;	PUNCT
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eurjchem-1700	218	7	,	,	PUNCT
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eurjchem-1700	218	12	.	.	PUNCT
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eurjchem-1700	219	2	.	.	PROPN
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eurjchem-1700	219	4	,	,	PUNCT
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eurjchem-1700	219	6	,	,	PUNCT
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eurjchem-1700	219	8	-	-	SYM
eurjchem-1700	219	9	856	856	NUM
eurjchem-1700	219	10	.	.	PUNCT
eurjchem-1700	220	1	[	[	X
eurjchem-1700	220	2	12	12	NUM
eurjchem-1700	220	3	]	]	PUNCT
eurjchem-1700	220	4	.	.	PUNCT
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eurjchem-1700	221	2	,	,	PUNCT
eurjchem-1700	221	3	p.	p.	PROPN
eurjchem-1700	221	4	b.	b.	PROPN
eurjchem-1700	221	5	;	;	PUNCT
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eurjchem-1700	221	7	,	,	PUNCT
eurjchem-1700	221	8	p.	p.	PROPN
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eurjchem-1700	221	10	;	;	PUNCT
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eurjchem-1700	221	17	,	,	PUNCT
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eurjchem-1700	221	20	;	;	PUNCT
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eurjchem-1700	221	22	,	,	PUNCT
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eurjchem-1700	221	25	;	;	PUNCT
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eurjchem-1700	221	31	;	;	PUNCT
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eurjchem-1700	221	33	,	,	PUNCT
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eurjchem-1700	221	37	,	,	PUNCT
eurjchem-1700	221	38	n.	n.	NOUN
eurjchem-1700	221	39	;	;	PUNCT
eurjchem-1700	221	40	bairy	bairy	PROPN
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eurjchem-1700	222	2	,	,	PUNCT
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eurjchem-1700	222	4	,	,	PUNCT
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eurjchem-1700	222	6	-	-	SYM
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eurjchem-1700	222	8	.	.	PUNCT
eurjchem-1700	223	1	[	[	X
eurjchem-1700	223	2	13	13	NUM
eurjchem-1700	223	3	]	]	PUNCT
eurjchem-1700	223	4	.	.	PUNCT
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eurjchem-1700	224	2	,	,	PUNCT
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eurjchem-1700	224	4	;	;	PUNCT
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eurjchem-1700	224	6	,	,	PUNCT
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eurjchem-1700	224	14	,	,	PUNCT
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eurjchem-1700	224	18	,	,	PUNCT
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eurjchem-1700	224	20	,	,	PUNCT
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eurjchem-1700	224	22	-	-	SYM
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eurjchem-1700	224	24	.	.	PUNCT
eurjchem-1700	225	1	[	[	X
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eurjchem-1700	225	3	]	]	PUNCT
eurjchem-1700	225	4	.	.	PUNCT
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eurjchem-1700	230	10	.	.	PUNCT
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eurjchem-1700	231	2	©	©	PROPN
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eurjchem-1700	232	5	and	and	CCONJ
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eurjchem-1700	232	8	atlanta	atlanta	PROPN
eurjchem-1700	232	9	publishing	publishing	PROPN
eurjchem-1700	232	10	house	house	PROPN
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eurjchem-1700	232	12	,	,	PUNCT
eurjchem-1700	232	13	atlanta	atlanta	PROPN
eurjchem-1700	232	14	,	,	PUNCT
eurjchem-1700	232	15	ga	ga	PROPN
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eurjchem-1700	232	17	usa	usa	PROPN
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eurjchem-1700	233	4	of	of	ADP
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eurjchem-1700	233	15	commons	common	NOUN
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eurjchem-1700	233	20	(	(	PUNCT
eurjchem-1700	233	21	cc	cc	NOUN
eurjchem-1700	233	22	by	by	ADP
eurjchem-1700	233	23	nc	nc	PROPN
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eurjchem-1700	233	25	(	(	PUNCT
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eurjchem-1700	233	31	(	(	PUNCT
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eurjchem-1700	234	9	the	the	DET
eurjchem-1700	234	10	terms	term	NOUN
eurjchem-1700	234	11	.	.	PUNCT
eurjchem-1700	235	1	this	this	PRON
eurjchem-1700	235	2	is	be	AUX
eurjchem-1700	235	3	an	an	DET
eurjchem-1700	235	4	open	open	ADJ
eurjchem-1700	235	5	access	access	NOUN
eurjchem-1700	235	6	article	article	NOUN
eurjchem-1700	235	7	distributed	distribute	VERB
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eurjchem-1700	235	9	the	the	DET
eurjchem-1700	235	10	terms	term	NOUN
eurjchem-1700	235	11	and	and	CCONJ
eurjchem-1700	235	12	conditions	condition	NOUN
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eurjchem-1700	235	15	cc	cc	PROPN
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eurjchem-1700	235	29	,	,	PUNCT
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eurjchem-1700	235	32	in	in	ADP
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eurjchem-1700	235	49	publishing	publishing	PROPN
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eurjchem-1700	235	51	llc	llc	PROPN
eurjchem-1700	235	52	(	(	PUNCT
eurjchem-1700	235	53	european	european	PROPN
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eurjchem-1700	235	57	)	)	PUNCT
eurjchem-1700	235	58	.	.	PUNCT
eurjchem-1700	236	1	no	no	DET
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eurjchem-1700	236	3	,	,	PUNCT
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eurjchem-1700	236	15	terms	term	NOUN
eurjchem-1700	236	16	.	.	PUNCT
eurjchem-1700	237	1	permissions	permission	NOUN
eurjchem-1700	237	2	for	for	ADP
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eurjchem-1700	237	14	(	(	PUNCT
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eurjchem-1700	237	16	)	)	PUNCT
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eurjchem-1700	237	21	publishing	publishing	PROPN
eurjchem-1700	237	22	house	house	PROPN
eurjchem-1700	237	23	llc	llc	PROPN
eurjchem-1700	237	24	(	(	PUNCT
eurjchem-1700	237	25	european	european	PROPN
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eurjchem-1700	238	7	–	–	PUNCT
eurjchem-1700	238	8	cc	cc	NOUN
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eurjchem-1700	238	10	nc	nc	PROPN
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eurjchem-1700	238	22	http://orcid.org/0000-0001-6186-9234	http://orcid.org/0000-0001-6186-9234	ADJ
eurjchem-1700	238	23	http://www.eurjchem.com/index.php/eurjchem/pages/view/terms	http://www.eurjchem.com/index.php/eurjchem/pages/view/term	NOUN
eurjchem-1700	238	24	http://creativecommons.org/licenses/by-nc/4.0	http://creativecommons.org/licenses/by-nc/4.0	PROPN
eurjchem-1700	238	25	http://www.eurjchem.com/index.php/eurjchem/pages/view/terms	http://www.eurjchem.com/index.php/eurjchem/pages/view/terms	PROPN
eurjchem-1700	238	26	1	1	NUM
eurjchem-1700	238	27	.	.	PUNCT
eurjchem-1700	238	28	introduction	introduction	NOUN
eurjchem-1700	238	29	2	2	NUM
eurjchem-1700	238	30	.	.	PUNCT
eurjchem-1700	238	31	experimental	experimental	ADJ
eurjchem-1700	238	32	2.1	2.1	NUM
eurjchem-1700	238	33	.	.	PUNCT
eurjchem-1700	239	1	materials	material	NOUN
eurjchem-1700	239	2	2.2	2.2	NUM
eurjchem-1700	239	3	.	.	PUNCT
eurjchem-1700	240	1	equipments	equipment	NOUN
eurjchem-1700	240	2	and	and	CCONJ
eurjchem-1700	240	3	chromatographic	chromatographic	ADJ
eurjchem-1700	240	4	conditions	condition	NOUN
eurjchem-1700	240	5	2.3	2.3	NUM
eurjchem-1700	240	6	.	.	PUNCT
eurjchem-1700	241	1	preparation	preparation	NOUN
eurjchem-1700	241	2	of	of	ADP
eurjchem-1700	241	3	standard	standard	ADJ
eurjchem-1700	241	4	solution	solution	NOUN
eurjchem-1700	241	5	2.4	2.4	NUM
eurjchem-1700	241	6	.	.	PUNCT
eurjchem-1700	242	1	preparation	preparation	NOUN
eurjchem-1700	242	2	of	of	ADP
eurjchem-1700	242	3	sample	sample	NOUN
eurjchem-1700	242	4	solution	solution	NOUN
eurjchem-1700	242	5	2.5	2.5	NUM
eurjchem-1700	242	6	.	.	PUNCT
eurjchem-1700	243	1	method	method	VERB
eurjchem-1700	243	2	validation	validation	NOUN
eurjchem-1700	243	3	2.5.1	2.5.1	NUM
eurjchem-1700	243	4	.	.	PUNCT
eurjchem-1700	244	1	system	system	NOUN
eurjchem-1700	244	2	suitability	suitability	NOUN
eurjchem-1700	244	3	2.5.2	2.5.2	NUM
eurjchem-1700	244	4	.	.	PUNCT
eurjchem-1700	245	1	linearity	linearity	PROPN
eurjchem-1700	245	2	2.5.3	2.5.3	NUM
eurjchem-1700	245	3	.	.	PUNCT
eurjchem-1700	245	4	precision	precision	PROPN
eurjchem-1700	245	5	2.5.4	2.5.4	NUM
eurjchem-1700	245	6	.	.	PUNCT
eurjchem-1700	246	1	accuracy	accuracy	NOUN
eurjchem-1700	246	2	2.5.5	2.5.5	NUM
eurjchem-1700	246	3	.	.	PUNCT
eurjchem-1700	247	1	limit	limit	NOUN
eurjchem-1700	247	2	of	of	ADP
eurjchem-1700	247	3	detection	detection	NOUN
eurjchem-1700	247	4	and	and	CCONJ
eurjchem-1700	247	5	limit	limit	NOUN
eurjchem-1700	247	6	of	of	ADP
eurjchem-1700	247	7	quantitation	quantitation	NOUN
eurjchem-1700	247	8	2.5.6	2.5.6	NUM
eurjchem-1700	247	9	.	.	PUNCT
eurjchem-1700	248	1	solution	solution	NOUN
eurjchem-1700	248	2	stability	stability	NOUN
eurjchem-1700	248	3	2.5.7	2.5.7	NUM
eurjchem-1700	248	4	.	.	PUNCT
eurjchem-1700	249	1	specificity	specificity	NOUN
eurjchem-1700	249	2	-	-	PUNCT
eurjchem-1700	249	3	forced	force	VERB
eurjchem-1700	249	4	degradation	degradation	NOUN
eurjchem-1700	249	5	studies	study	NOUN
eurjchem-1700	249	6	3	3	NUM
eurjchem-1700	249	7	.	.	NOUN
eurjchem-1700	249	8	results	result	NOUN
eurjchem-1700	249	9	and	and	CCONJ
eurjchem-1700	249	10	discussion	discussion	NOUN
eurjchem-1700	249	11	3.1	3.1	NUM
eurjchem-1700	249	12	.	.	PUNCT
eurjchem-1700	250	1	method	method	NOUN
eurjchem-1700	250	2	development	development	NOUN
eurjchem-1700	250	3	and	and	CCONJ
eurjchem-1700	250	4	optimization	optimization	NOUN
eurjchem-1700	250	5	3.2	3.2	NUM
eurjchem-1700	250	6	.	.	PUNCT
eurjchem-1700	251	1	method	method	NOUN
eurjchem-1700	251	2	validation	validation	NOUN
eurjchem-1700	251	3	4	4	NUM
eurjchem-1700	251	4	.	.	PUNCT
eurjchem-1700	252	1	conclusion	conclusion	NOUN
eurjchem-1700	252	2	disclosure	disclosure	NOUN
eurjchem-1700	252	3	statement	statement	NOUN
eurjchem-1700	252	4	orcid	orcid	PROPN
eurjchem-1700	252	5	references	reference	NOUN
eurjchem-1700	252	6	printfield10	printfield10	NOUN
eurjchem-1700	252	7	:	:	PUNCT
eurjchem-1700	252	8	printfield11	printfield11	NOUN
eurjchem-1700	252	9	:	:	PUNCT
eurjchem-1700	252	10	printfield12	printfield12	PROPN
eurjchem-1700	252	11	:	:	PUNCT
eurjchem-1700	252	12	printfield13	printfield13	VERB
eurjchem-1700	252	13	:	:	PUNCT
eurjchem-1700	252	14	printfield14	printfield14	NOUN
eurjchem-1700	252	15	:	:	PUNCT
eurjchem-1700	252	16	printfield15	printfield15	NOUN
eurjchem-1700	252	17	:	:	PUNCT
eurjchem-1700	252	18	printfield16	printfield16	ADJ
eurjchem-1700	252	19	:	:	PUNCT
eurjchem-1700	252	20	printfield20	printfield20	VERB
eurjchem-1700	252	21	:	:	PUNCT
eurjchem-1700	252	22	printfield21	printfield21	ADJ
eurjchem-1700	252	23	:	:	PUNCT
eurjchem-1700	252	24	printfield22	printfield22	NOUN
eurjchem-1700	252	25	:	:	PUNCT
eurjchem-1700	252	26	printfield23	printfield23	NOUN
eurjchem-1700	252	27	:	:	PUNCT
eurjchem-1700	252	28	printfield24	printfield24	NOUN
eurjchem-1700	252	29	:	:	PUNCT
eurjchem-1700	252	30	printfield25	printfield25	NOUN
eurjchem-1700	252	31	:	:	PUNCT
eurjchem-1700	252	32	printfield26	printfield26	ADJ
eurjchem-1700	252	33	:	:	PUNCT