id	sid	tid	token	lemma	pos
eurjchem-1701	1	1	a	a	DET
eurjchem-1701	1	2	series	series	NOUN
eurjchem-1701	1	3	of	of	ADP
eurjchem-1701	1	4	1,3	1,3	NUM
eurjchem-1701	1	5	-	-	PUNCT
eurjchem-1701	1	6	imidazoles	imidazole	NOUN
eurjchem-1701	1	7	and	and	CCONJ
eurjchem-1701	1	8	triazole-3	triazole-3	NOUN
eurjchem-1701	1	9	-	-	PUNCT
eurjchem-1701	1	10	thiones	thione	NOUN
eurjchem-1701	1	11	based	base	VERB
eurjchem-1701	1	12	thiophene-2	thiophene-2	NOUN
eurjchem-1701	1	13	-	-	NOUN
eurjchem-1701	1	14	carboxamides	carboxamide	VERB
eurjchem-1701	1	15	as	as	ADP
eurjchem-1701	1	16	anticancer	anticancer	NOUN
eurjchem-1701	1	17	agents	agent	NOUN
eurjchem-1701	1	18	:	:	PUNCT
eurjchem-1701	1	19	synthesis	synthesis	NOUN
eurjchem-1701	1	20	and	and	CCONJ
eurjchem-1701	1	21	anticancer	anticancer	NOUN
eurjchem-1701	1	22	activity	activity	NOUN
eurjchem-1701	1	23	european	european	PROPN
eurjchem-1701	1	24	journal	journal	PROPN
eurjchem-1701	1	25	of	of	ADP
eurjchem-1701	1	26	chemistry	chemistry	NOUN
eurjchem-1701	1	27	9	9	NUM
eurjchem-1701	1	28	(	(	PUNCT
eurjchem-1701	1	29	2	2	NUM
eurjchem-1701	1	30	)	)	PUNCT
eurjchem-1701	1	31	(	(	PUNCT
eurjchem-1701	1	32	2018	2018	NUM
eurjchem-1701	1	33	)	)	PUNCT
eurjchem-1701	1	34	99	99	NUM
eurjchem-1701	1	35	-	-	SYM
eurjchem-1701	1	36	106	106	NUM
eurjchem-1701	1	37	european	european	ADJ
eurjchem-1701	1	38	journal	journal	PROPN
eurjchem-1701	1	39	of	of	ADP
eurjchem-1701	1	40	chemistry	chemistry	NOUN
eurjchem-1701	1	41	view	view	NOUN
eurjchem-1701	1	42	journal	journal	PROPN
eurjchem-1701	1	43	online	online	PROPN
eurjchem-1701	1	44	view	view	NOUN
eurjchem-1701	1	45	article	article	NOUN
eurjchem-1701	1	46	online	online	ADV
eurjchem-1701	1	47	a	a	DET
eurjchem-1701	1	48	series	series	NOUN
eurjchem-1701	1	49	of	of	ADP
eurjchem-1701	1	50	1,3	1,3	NUM
eurjchem-1701	1	51	-	-	PUNCT
eurjchem-1701	1	52	imidazoles	imidazole	NOUN
eurjchem-1701	1	53	and	and	CCONJ
eurjchem-1701	1	54	triazole-3	triazole-3	NOUN
eurjchem-1701	1	55	-	-	PUNCT
eurjchem-1701	1	56	thiones	thione	NOUN
eurjchem-1701	1	57	based	base	VERB
eurjchem-1701	1	58	thiophene-2carboxamides	thiophene-2carboxamides	PROPN
eurjchem-1701	1	59	as	as	ADP
eurjchem-1701	1	60	anticancer	anticancer	NOUN
eurjchem-1701	1	61	agents	agent	NOUN
eurjchem-1701	1	62	:	:	PUNCT
eurjchem-1701	1	63	synthesis	synthesis	NOUN
eurjchem-1701	1	64	and	and	CCONJ
eurjchem-1701	1	65	anticancer	anticancer	NOUN
eurjchem-1701	1	66	activity	activity	NOUN
eurjchem-1701	1	67	reda	reda	PROPN
eurjchem-1701	1	68	ahmed	ahme	VERB
eurjchem-1701	1	69	haggam	haggam	PROPN
eurjchem-1701	1	70	1,2	1,2	NUM
eurjchem-1701	1	71	,	,	PUNCT
eurjchem-1701	1	72	*	*	PROPN
eurjchem-1701	1	73	,	,	PUNCT
eurjchem-1701	1	74	mohamed	mohamed	PROPN
eurjchem-1701	1	75	gomma	gomma	PROPN
eurjchem-1701	1	76	assy	assy	PROPN
eurjchem-1701	1	77	2	2	NUM
eurjchem-1701	1	78	,	,	PUNCT
eurjchem-1701	1	79	mohamed	mohamed	PROPN
eurjchem-1701	1	80	hassan	hassan	PROPN
eurjchem-1701	1	81	sherif	sherif	VERB
eurjchem-1701	1	82	2	2	PROPN
eurjchem-1701	1	83	and	and	CCONJ
eurjchem-1701	1	84	mohamed	mohamed	PROPN
eurjchem-1701	1	85	mohamed	mohamed	PROPN
eurjchem-1701	1	86	galahom	galahom	ADJ
eurjchem-1701	1	87	2	2	NUM
eurjchem-1701	1	88	1	1	NUM
eurjchem-1701	1	89	department	department	NOUN
eurjchem-1701	1	90	of	of	ADP
eurjchem-1701	1	91	chemistry	chemistry	NOUN
eurjchem-1701	1	92	,	,	PUNCT
eurjchem-1701	1	93	faculty	faculty	NOUN
eurjchem-1701	1	94	of	of	ADP
eurjchem-1701	1	95	science	science	NOUN
eurjchem-1701	1	96	,	,	PUNCT
eurjchem-1701	1	97	islamic	islamic	PROPN
eurjchem-1701	1	98	university	university	PROPN
eurjchem-1701	1	99	in	in	ADP
eurjchem-1701	1	100	madinah	madinah	PROPN
eurjchem-1701	1	101	,	,	PUNCT
eurjchem-1701	1	102	madinah	madinah	PROPN
eurjchem-1701	1	103	,	,	PUNCT
eurjchem-1701	1	104	42351	42351	NUM
eurjchem-1701	1	105	,	,	PUNCT
eurjchem-1701	1	106	kingdom	kingdom	NOUN
eurjchem-1701	1	107	of	of	ADP
eurjchem-1701	1	108	saudi	saudi	PROPN
eurjchem-1701	1	109	arabia	arabia	PROPN
eurjchem-1701	2	1	rhaggan99@hotmail.com	rhaggan99@hotmail.com	X
eurjchem-1701	2	2	(	(	PUNCT
eurjchem-1701	2	3	r.a.h	r.a.h	NOUN
eurjchem-1701	2	4	.	.	PUNCT
eurjchem-1701	2	5	)	)	PUNCT
eurjchem-1701	3	1	2	2	NUM
eurjchem-1701	3	2	department	department	NOUN
eurjchem-1701	3	3	of	of	ADP
eurjchem-1701	3	4	chemistry	chemistry	NOUN
eurjchem-1701	3	5	,	,	PUNCT
eurjchem-1701	3	6	faculty	faculty	NOUN
eurjchem-1701	3	7	of	of	ADP
eurjchem-1701	3	8	science	science	NOUN
eurjchem-1701	3	9	,	,	PUNCT
eurjchem-1701	3	10	university	university	PROPN
eurjchem-1701	3	11	of	of	ADP
eurjchem-1701	3	12	zagazig	zagazig	PROPN
eurjchem-1701	3	13	,	,	PUNCT
eurjchem-1701	3	14	zagazig	zagazig	PROPN
eurjchem-1701	3	15	,	,	PUNCT
eurjchem-1701	3	16	44519	44519	NUM
eurjchem-1701	3	17	,	,	PUNCT
eurjchem-1701	3	18	egypt	egypt	PROPN
eurjchem-1701	3	19	m_gomaa59@yahoo.com	m_gomaa59@yahoo.com	PROPN
eurjchem-1701	3	20	(	(	PUNCT
eurjchem-1701	3	21	m.g.a	m.g.a	NOUN
eurjchem-1701	3	22	.	.	PUNCT
eurjchem-1701	3	23	)	)	PUNCT
eurjchem-1701	3	24	,	,	PUNCT
eurjchem-1701	3	25	mohasherif@yahoo.com	mohasherif@yahoo.com	X
eurjchem-1701	3	26	(	(	PUNCT
eurjchem-1701	3	27	m.h.s	m.h.s	ADJ
eurjchem-1701	3	28	.	.	PUNCT
eurjchem-1701	3	29	)	)	PUNCT
eurjchem-1701	3	30	,	,	PUNCT
eurjchem-1701	3	31	mgalahom@yahoo.com	mgalahom@yahoo.com	X
eurjchem-1701	3	32	(	(	PUNCT
eurjchem-1701	3	33	m.m.g	m.m.g	ADJ
eurjchem-1701	3	34	.	.	PUNCT
eurjchem-1701	3	35	)	)	PUNCT
eurjchem-1701	4	1	*	*	PUNCT
eurjchem-1701	4	2	corresponding	correspond	VERB
eurjchem-1701	4	3	author	author	NOUN
eurjchem-1701	4	4	at	at	ADP
eurjchem-1701	4	5	:	:	PUNCT
eurjchem-1701	4	6	department	department	NOUN
eurjchem-1701	4	7	of	of	ADP
eurjchem-1701	4	8	chemistry	chemistry	NOUN
eurjchem-1701	4	9	,	,	PUNCT
eurjchem-1701	4	10	faculty	faculty	NOUN
eurjchem-1701	4	11	of	of	ADP
eurjchem-1701	4	12	science	science	NOUN
eurjchem-1701	4	13	,	,	PUNCT
eurjchem-1701	4	14	islamic	islamic	PROPN
eurjchem-1701	4	15	university	university	PROPN
eurjchem-1701	4	16	in	in	ADP
eurjchem-1701	4	17	madinah	madinah	PROPN
eurjchem-1701	4	18	,	,	PUNCT
eurjchem-1701	4	19	madinah	madinah	PROPN
eurjchem-1701	4	20	,	,	PUNCT
eurjchem-1701	4	21	42351	42351	NUM
eurjchem-1701	4	22	,	,	PUNCT
eurjchem-1701	4	23	kingdom	kingdom	NOUN
eurjchem-1701	4	24	of	of	ADP
eurjchem-1701	4	25	saudi	saudi	PROPN
eurjchem-1701	4	26	arabia	arabia	PROPN
eurjchem-1701	4	27	.	.	PUNCT
eurjchem-1701	5	1	tel	tel	ADP
eurjchem-1701	5	2	:	:	PUNCT
eurjchem-1701	5	3	+966.014.537587227	+966.014.537587227	NUM
eurjchem-1701	5	4	fax	fax	NOUN
eurjchem-1701	5	5	:	:	PUNCT
eurjchem-1701	5	6	+966.014.8470354	+966.014.8470354	PRON
eurjchem-1701	5	7	e	e	NOUN
eurjchem-1701	5	8	-	-	NOUN
eurjchem-1701	5	9	mail	mail	NOUN
eurjchem-1701	5	10	:	:	PUNCT
eurjchem-1701	6	1	rhaggan99@hotmail.com	rhaggan99@hotmail.com	PROPN
eurjchem-1701	6	2	(	(	PUNCT
eurjchem-1701	6	3	r.a	r.a	PROPN
eurjchem-1701	6	4	.	.	PROPN
eurjchem-1701	6	5	haggam	haggam	PROPN
eurjchem-1701	6	6	)	)	PUNCT
eurjchem-1701	6	7	.	.	PUNCT
eurjchem-1701	7	1	10.5155	10.5155	NUM
eurjchem-1701	7	2	/	/	SYM
eurjchem-1701	7	3	eurjchem.9.2.99	eurjchem.9.2.99	NUM
eurjchem-1701	7	4	-	-	PUNCT
eurjchem-1701	7	5	106.1701	106.1701	NUM
eurjchem-1701	7	6	received	receive	VERB
eurjchem-1701	7	7	:	:	PUNCT
eurjchem-1701	7	8	18	18	NUM
eurjchem-1701	7	9	march	march	NOUN
eurjchem-1701	7	10	2018	2018	NUM
eurjchem-1701	7	11	received	receive	VERB
eurjchem-1701	7	12	in	in	ADP
eurjchem-1701	7	13	revised	revise	VERB
eurjchem-1701	7	14	form	form	NOUN
eurjchem-1701	7	15	:	:	PUNCT
eurjchem-1701	7	16	09	09	NUM
eurjchem-1701	7	17	april	april	PROPN
eurjchem-1701	7	18	2018	2018	NUM
eurjchem-1701	7	19	accepted	accept	VERB
eurjchem-1701	7	20	:	:	PUNCT
eurjchem-1701	7	21	16	16	NUM
eurjchem-1701	7	22	april	april	PROPN
eurjchem-1701	7	23	2018	2018	NUM
eurjchem-1701	7	24	published	publish	VERB
eurjchem-1701	7	25	online	online	ADV
eurjchem-1701	7	26	:	:	PUNCT
eurjchem-1701	7	27	30	30	NUM
eurjchem-1701	7	28	june	june	PROPN
eurjchem-1701	7	29	2018	2018	NUM
eurjchem-1701	7	30	printed	print	VERB
eurjchem-1701	7	31	:	:	PUNCT
eurjchem-1701	7	32	30	30	NUM
eurjchem-1701	7	33	june	june	PROPN
eurjchem-1701	7	34	2018	2018	NUM
eurjchem-1701	7	35	by	by	ADP
eurjchem-1701	7	36	addition	addition	NOUN
eurjchem-1701	7	37	of	of	ADP
eurjchem-1701	7	38	semicarbazide	semicarbazide	NOUN
eurjchem-1701	7	39	or	or	CCONJ
eurjchem-1701	7	40	phenylhydrazine	phenylhydrazine	VERB
eurjchem-1701	7	41	hydrochloride	hydrochloride	NOUN
eurjchem-1701	7	42	to	to	ADP
eurjchem-1701	7	43	thienoylisothiocyanate	thienoylisothiocyanate	NOUN
eurjchem-1701	7	44	(	(	PUNCT
eurjchem-1701	7	45	1	1	NUM
eurjchem-1701	7	46	)	)	PUNCT
eurjchem-1701	7	47	resulted	result	VERB
eurjchem-1701	7	48	in	in	ADP
eurjchem-1701	7	49	building	building	NOUN
eurjchem-1701	7	50	of	of	ADP
eurjchem-1701	7	51	thiosemicarbazide	thiosemicarbazide	ADJ
eurjchem-1701	7	52	derivative	derivative	NOUN
eurjchem-1701	7	53	(	(	PUNCT
eurjchem-1701	7	54	2	2	NUM
eurjchem-1701	7	55	)	)	PUNCT
eurjchem-1701	7	56	,	,	PUNCT
eurjchem-1701	8	1	triazole	triazole	NOUN
eurjchem-1701	8	2	derivative	derivative	NOUN
eurjchem-1701	8	3	(	(	PUNCT
eurjchem-1701	8	4	4	4	NUM
eurjchem-1701	8	5	)	)	PUNCT
eurjchem-1701	8	6	and	and	CCONJ
eurjchem-1701	8	7	thiophene-2	thiophene-2	NUM
eurjchem-1701	8	8	-	-	NOUN
eurjchem-1701	8	9	carboxamide	carboxamide	NOUN
eurjchem-1701	8	10	(	(	PUNCT
eurjchem-1701	8	11	5	5	NUM
eurjchem-1701	8	12	)	)	PUNCT
eurjchem-1701	8	13	,	,	PUNCT
eurjchem-1701	8	14	respectively	respectively	ADV
eurjchem-1701	8	15	.	.	PUNCT
eurjchem-1701	9	1	basic	basic	ADJ
eurjchem-1701	9	2	cyclization	cyclization	NOUN
eurjchem-1701	9	3	of	of	ADP
eurjchem-1701	9	4	compound	compound	NOUN
eurjchem-1701	9	5	2	2	NUM
eurjchem-1701	9	6	led	lead	VERB
eurjchem-1701	9	7	to	to	ADP
eurjchem-1701	9	8	formation	formation	NOUN
eurjchem-1701	9	9	of	of	ADP
eurjchem-1701	9	10	oxadiazine	oxadiazine	NOUN
eurjchem-1701	9	11	(	(	PUNCT
eurjchem-1701	9	12	3	3	NUM
eurjchem-1701	9	13	)	)	PUNCT
eurjchem-1701	9	14	.	.	PUNCT
eurjchem-1701	10	1	synthesis	synthesis	NOUN
eurjchem-1701	10	2	of	of	ADP
eurjchem-1701	10	3	thiadiazine	thiadiazine	ADJ
eurjchem-1701	10	4	derivative	derivative	ADJ
eurjchem-1701	10	5	(	(	PUNCT
eurjchem-1701	10	6	6	6	NUM
eurjchem-1701	10	7	)	)	PUNCT
eurjchem-1701	10	8	was	be	AUX
eurjchem-1701	10	9	achieved	achieve	VERB
eurjchem-1701	10	10	via	via	ADP
eurjchem-1701	10	11	reaction	reaction	NOUN
eurjchem-1701	10	12	of	of	ADP
eurjchem-1701	10	13	compound	compound	NOUN
eurjchem-1701	10	14	5	5	NUM
eurjchem-1701	10	15	and	and	CCONJ
eurjchem-1701	10	16	maleic	maleic	VERB
eurjchem-1701	10	17	anhydride	anhydride	NOUN
eurjchem-1701	10	18	in	in	ADP
eurjchem-1701	10	19	triethyl	triethyl	PROPN
eurjchem-1701	10	20	amine	amine	PROPN
eurjchem-1701	10	21	.	.	PUNCT
eurjchem-1701	11	1	heating	heating	NOUN
eurjchem-1701	11	2	of	of	ADP
eurjchem-1701	11	3	compound	compound	NOUN
eurjchem-1701	11	4	5	5	NUM
eurjchem-1701	11	5	with	with	ADP
eurjchem-1701	11	6	ethyl	ethyl	PROPN
eurjchem-1701	11	7	chloroacetate	chloroacetate	NOUN
eurjchem-1701	11	8	or	or	CCONJ
eurjchem-1701	11	9	sodium	sodium	NOUN
eurjchem-1701	11	10	ethoxide	ethoxide	NOUN
eurjchem-1701	11	11	produced	produce	VERB
eurjchem-1701	11	12	thiadiazine	thiadiazine	NOUN
eurjchem-1701	11	13	derivative	derivative	NOUN
eurjchem-1701	11	14	(	(	PUNCT
eurjchem-1701	11	15	7	7	NUM
eurjchem-1701	11	16	)	)	PUNCT
eurjchem-1701	11	17	and	and	CCONJ
eurjchem-1701	11	18	triazolethione	triazolethione	NOUN
eurjchem-1701	11	19	(	(	PUNCT
eurjchem-1701	11	20	8)	8)	NUM
eurjchem-1701	11	21	,	,	PUNCT
eurjchem-1701	11	22	respectively	respectively	ADV
eurjchem-1701	11	23	.	.	PUNCT
eurjchem-1701	12	1	thiosemicarbazide	thiosemicarbazide	VERB
eurjchem-1701	12	2	derivative	derivative	ADJ
eurjchem-1701	12	3	11	11	NUM
eurjchem-1701	12	4	was	be	AUX
eurjchem-1701	12	5	synthesized	synthesize	VERB
eurjchem-1701	12	6	by	by	ADP
eurjchem-1701	12	7	addition	addition	NOUN
eurjchem-1701	12	8	of	of	ADP
eurjchem-1701	12	9	nicotinic	nicotinic	ADJ
eurjchem-1701	12	10	hydrazide	hydrazide	NOUN
eurjchem-1701	12	11	to	to	PART
eurjchem-1701	12	12	compound	compound	VERB
eurjchem-1701	12	13	1	1	NUM
eurjchem-1701	12	14	.	.	PUNCT
eurjchem-1701	13	1	refluxing	refluxing	NOUN
eurjchem-1701	13	2	of	of	ADP
eurjchem-1701	13	3	compound	compound	NOUN
eurjchem-1701	13	4	11	11	NUM
eurjchem-1701	13	5	with	with	ADP
eurjchem-1701	13	6	lead	lead	ADJ
eurjchem-1701	13	7	acetate	acetate	NOUN
eurjchem-1701	13	8	afforded	afford	VERB
eurjchem-1701	13	9	triazole	triazole	NOUN
eurjchem-1701	13	10	(	(	PUNCT
eurjchem-1701	13	11	13	13	NUM
eurjchem-1701	13	12	)	)	PUNCT
eurjchem-1701	13	13	.	.	PUNCT
eurjchem-1701	14	1	moreover	moreover	ADV
eurjchem-1701	14	2	,	,	PUNCT
eurjchem-1701	14	3	acid	acid	ADJ
eurjchem-1701	14	4	and	and	CCONJ
eurjchem-1701	14	5	base	base	NOUN
eurjchem-1701	14	6	mediated	mediate	VERB
eurjchem-1701	14	7	cyclizations	cyclization	NOUN
eurjchem-1701	14	8	of	of	ADP
eurjchem-1701	14	9	compound	compound	NOUN
eurjchem-1701	14	10	11	11	NUM
eurjchem-1701	14	11	gave	give	VERB
eurjchem-1701	14	12	thiadiazole	thiadiazole	NOUN
eurjchem-1701	14	13	(	(	PUNCT
eurjchem-1701	14	14	12	12	NUM
eurjchem-1701	14	15	)	)	PUNCT
eurjchem-1701	14	16	and	and	CCONJ
eurjchem-1701	14	17	1,2,4	1,2,4	NUM
eurjchem-1701	14	18	-	-	PUNCT
eurjchem-1701	14	19	triazolethione	triazolethione	NOUN
eurjchem-1701	14	20	(	(	PUNCT
eurjchem-1701	14	21	14	14	NUM
eurjchem-1701	14	22	)	)	PUNCT
eurjchem-1701	14	23	throughout	throughout	ADP
eurjchem-1701	14	24	thiophene	thiophene	NOUN
eurjchem-1701	14	25	intermediate	intermediate	ADJ
eurjchem-1701	14	26	,	,	PUNCT
eurjchem-1701	14	27	respectively	respectively	ADV
eurjchem-1701	14	28	.	.	PUNCT
eurjchem-1701	15	1	addition	addition	NOUN
eurjchem-1701	15	2	of	of	ADP
eurjchem-1701	15	3	ethyl	ethyl	PROPN
eurjchem-1701	15	4	2	2	NUM
eurjchem-1701	15	5	-	-	PUNCT
eurjchem-1701	15	6	aminothiophene-3	aminothiophene-3	NUM
eurjchem-1701	15	7	-	-	NOUN
eurjchem-1701	15	8	carboxylate	carboxylate	NOUN
eurjchem-1701	15	9	to	to	PART
eurjchem-1701	15	10	compound	compound	VERB
eurjchem-1701	15	11	1	1	NUM
eurjchem-1701	15	12	formed	form	VERB
eurjchem-1701	15	13	thiourea	thiourea	NOUN
eurjchem-1701	15	14	(	(	PUNCT
eurjchem-1701	15	15	15	15	NUM
eurjchem-1701	15	16	)	)	PUNCT
eurjchem-1701	15	17	which	which	PRON
eurjchem-1701	15	18	was	be	AUX
eurjchem-1701	15	19	refluxed	refluxe	VERB
eurjchem-1701	15	20	with	with	ADP
eurjchem-1701	15	21	ethoxide	ethoxide	NOUN
eurjchem-1701	15	22	giving	give	VERB
eurjchem-1701	15	23	thiophene-3	thiophene-3	NUM
eurjchem-1701	15	24	-	-	PUNCT
eurjchem-1701	15	25	carboxylic	carboxylic	ADJ
eurjchem-1701	15	26	acid	acid	NOUN
eurjchem-1701	15	27	(	(	PUNCT
eurjchem-1701	15	28	16	16	NUM
eurjchem-1701	15	29	)	)	PUNCT
eurjchem-1701	15	30	.	.	PUNCT
eurjchem-1701	16	1	lastly	lastly	ADV
eurjchem-1701	16	2	,	,	PUNCT
eurjchem-1701	16	3	nucleophilic	nucleophilic	ADJ
eurjchem-1701	16	4	addition	addition	NOUN
eurjchem-1701	16	5	of	of	ADP
eurjchem-1701	16	6	amino	amino	ADJ
eurjchem-1701	16	7	phenol	phenol	NOUN
eurjchem-1701	16	8	or	or	CCONJ
eurjchem-1701	16	9	ethylene	ethylene	NOUN
eurjchem-1701	16	10	diamine	diamine	NOUN
eurjchem-1701	16	11	to	to	PART
eurjchem-1701	16	12	compound	compound	VERB
eurjchem-1701	16	13	1	1	NUM
eurjchem-1701	16	14	yielded	yield	VERB
eurjchem-1701	16	15	oxazine	oxazine	NOUN
eurjchem-1701	16	16	structure	structure	NOUN
eurjchem-1701	16	17	(	(	PUNCT
eurjchem-1701	16	18	18	18	NUM
eurjchem-1701	16	19	)	)	PUNCT
eurjchem-1701	16	20	and	and	CCONJ
eurjchem-1701	16	21	imidazole	imidazole	NOUN
eurjchem-1701	16	22	derivative	derivative	NOUN
eurjchem-1701	16	23	(	(	PUNCT
eurjchem-1701	16	24	19	19	NUM
eurjchem-1701	16	25	)	)	PUNCT
eurjchem-1701	16	26	,	,	PUNCT
eurjchem-1701	16	27	respectively	respectively	ADV
eurjchem-1701	16	28	.	.	PUNCT
eurjchem-1701	17	1	the	the	DET
eurjchem-1701	17	2	yields	yield	NOUN
eurjchem-1701	17	3	of	of	ADP
eurjchem-1701	17	4	the	the	DET
eurjchem-1701	17	5	synthesized	synthesize	VERB
eurjchem-1701	17	6	compounds	compound	NOUN
eurjchem-1701	17	7	were	be	AUX
eurjchem-1701	17	8	6195	6195	NUM
eurjchem-1701	17	9	%	%	NOUN
eurjchem-1701	17	10	.	.	PUNCT
eurjchem-1701	18	1	the	the	DET
eurjchem-1701	18	2	detailed	detailed	ADJ
eurjchem-1701	18	3	synthesis	synthesis	NOUN
eurjchem-1701	18	4	and	and	CCONJ
eurjchem-1701	18	5	spectroscopic	spectroscopic	ADJ
eurjchem-1701	18	6	data	datum	NOUN
eurjchem-1701	18	7	of	of	ADP
eurjchem-1701	18	8	the	the	DET
eurjchem-1701	18	9	new	new	ADJ
eurjchem-1701	18	10	compounds	compound	NOUN
eurjchem-1701	18	11	are	be	AUX
eurjchem-1701	18	12	reported	report	VERB
eurjchem-1701	18	13	.	.	PUNCT
eurjchem-1701	19	1	thiophene	thiophene	NOUN
eurjchem-1701	19	2	1,3	1,3	NUM
eurjchem-1701	19	3	-	-	PUNCT
eurjchem-1701	19	4	imidazole	imidazole	NOUN
eurjchem-1701	19	5	isothiocyanates	isothiocyanate	VERB
eurjchem-1701	19	6	1,3,4	1,3,4	NUM
eurjchem-1701	19	7	-	-	PUNCT
eurjchem-1701	19	8	thiadiazoles	thiadiazole	NOUN
eurjchem-1701	19	9	triazole-3	triazole-3	NOUN
eurjchem-1701	19	10	-	-	PUNCT
eurjchem-1701	19	11	thiones	thione	NOUN
eurjchem-1701	19	12	anticancer	anticancer	NOUN
eurjchem-1701	19	13	activity	activity	NOUN
eurjchem-1701	19	14	cite	cite	VERB
eurjchem-1701	19	15	this	this	PRON
eurjchem-1701	19	16	:	:	PUNCT
eurjchem-1701	19	17	eur	eur	PROPN
eurjchem-1701	19	18	.	.	PUNCT
eurjchem-1701	20	1	j.	j.	PROPN
eurjchem-1701	20	2	chem	chem	PROPN
eurjchem-1701	20	3	.	.	PUNCT
eurjchem-1701	21	1	2018	2018	NUM
eurjchem-1701	21	2	,	,	PUNCT
eurjchem-1701	21	3	9(2	9(2	NUM
eurjchem-1701	21	4	)	)	PUNCT
eurjchem-1701	21	5	,	,	PUNCT
eurjchem-1701	21	6	99	99	NUM
eurjchem-1701	21	7	-	-	SYM
eurjchem-1701	21	8	106	106	NUM
eurjchem-1701	21	9	journal	journal	NOUN
eurjchem-1701	21	10	website	website	NOUN
eurjchem-1701	21	11	:	:	PUNCT
eurjchem-1701	21	12	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1701	21	13	1	1	X
eurjchem-1701	21	14	.	.	PUNCT
eurjchem-1701	21	15	introduction	introduction	NOUN
eurjchem-1701	21	16	aromatic	aromatic	ADJ
eurjchem-1701	21	17	five	five	NUM
eurjchem-1701	21	18	-	-	PUNCT
eurjchem-1701	21	19	membered	membere	VERB
eurjchem-1701	21	20	nitrogen	nitrogen	NOUN
eurjchem-1701	21	21	heterocycles	heterocycle	NOUN
eurjchem-1701	21	22	have	have	AUX
eurjchem-1701	21	23	been	be	AUX
eurjchem-1701	21	24	potential	potential	ADJ
eurjchem-1701	21	25	targets	target	NOUN
eurjchem-1701	21	26	of	of	ADP
eurjchem-1701	21	27	investigations	investigation	NOUN
eurjchem-1701	21	28	because	because	SCONJ
eurjchem-1701	21	29	of	of	ADP
eurjchem-1701	21	30	their	their	PRON
eurjchem-1701	21	31	medicinal	medicinal	ADJ
eurjchem-1701	21	32	properties	property	NOUN
eurjchem-1701	21	33	.	.	PUNCT
eurjchem-1701	22	1	in	in	ADP
eurjchem-1701	22	2	the	the	DET
eurjchem-1701	22	3	last	last	ADJ
eurjchem-1701	22	4	few	few	ADJ
eurjchem-1701	22	5	decades	decade	NOUN
eurjchem-1701	22	6	,	,	PUNCT
eurjchem-1701	22	7	the	the	DET
eurjchem-1701	22	8	chemistry	chemistry	NOUN
eurjchem-1701	22	9	of	of	ADP
eurjchem-1701	22	10	1,2,4triazole-3	1,2,4triazole-3	NUM
eurjchem-1701	22	11	-	-	PUNCT
eurjchem-1701	22	12	thiones	thione	NOUN
eurjchem-1701	22	13	,	,	PUNCT
eurjchem-1701	22	14	1,3,4	1,3,4	NUM
eurjchem-1701	22	15	-	-	PUNCT
eurjchem-1701	22	16	thiadiazoles	thiadiazole	NOUN
eurjchem-1701	22	17	and	and	CCONJ
eurjchem-1701	22	18	their	their	PRON
eurjchem-1701	22	19	fused	fuse	VERB
eurjchem-1701	22	20	heterocyclic	heterocyclic	ADJ
eurjchem-1701	22	21	derivatives	derivative	NOUN
eurjchem-1701	22	22	has	have	AUX
eurjchem-1701	22	23	received	receive	VERB
eurjchem-1701	22	24	considerable	considerable	ADJ
eurjchem-1701	22	25	attention	attention	NOUN
eurjchem-1701	22	26	owing	owe	VERB
eurjchem-1701	22	27	to	to	ADP
eurjchem-1701	22	28	their	their	PRON
eurjchem-1701	22	29	effective	effective	ADJ
eurjchem-1701	22	30	biological	biological	ADJ
eurjchem-1701	22	31	activities	activity	NOUN
eurjchem-1701	22	32	as	as	ADP
eurjchem-1701	22	33	anticonvulsant	anticonvulsant	ADJ
eurjchem-1701	22	34	[	[	X
eurjchem-1701	22	35	1,2	1,2	NUM
eurjchem-1701	22	36	]	]	PUNCT
eurjchem-1701	22	37	and	and	CCONJ
eurjchem-1701	22	38	antioxidant	antioxidant	ADJ
eurjchem-1701	22	39	[	[	X
eurjchem-1701	22	40	3	3	NUM
eurjchem-1701	22	41	]	]	PUNCT
eurjchem-1701	22	42	.	.	PUNCT
eurjchem-1701	23	1	several	several	ADJ
eurjchem-1701	23	2	imidazole	imidazole	NOUN
eurjchem-1701	23	3	derivatives	derivative	NOUN
eurjchem-1701	23	4	have	have	AUX
eurjchem-1701	23	5	been	be	AUX
eurjchem-1701	23	6	published	publish	VERB
eurjchem-1701	23	7	as	as	ADP
eurjchem-1701	23	8	antiviral	antiviral	ADJ
eurjchem-1701	23	9	[	[	X
eurjchem-1701	23	10	4	4	NUM
eurjchem-1701	23	11	]	]	PUNCT
eurjchem-1701	23	12	,	,	PUNCT
eurjchem-1701	23	13	anticoagulant	anticoagulant	VERB
eurjchem-1701	23	14	[	[	X
eurjchem-1701	23	15	5	5	NUM
eurjchem-1701	23	16	]	]	PUNCT
eurjchem-1701	23	17	and	and	CCONJ
eurjchem-1701	23	18	anticancer	anticancer	NOUN
eurjchem-1701	24	1	[	[	X
eurjchem-1701	24	2	6,7	6,7	NUM
eurjchem-1701	24	3	]	]	PUNCT
eurjchem-1701	24	4	agents	agent	NOUN
eurjchem-1701	24	5	.	.	PUNCT
eurjchem-1701	25	1	the	the	DET
eurjchem-1701	25	2	1,2,4	1,2,4	NUM
eurjchem-1701	25	3	-	-	PUNCT
eurjchem-1701	25	4	triazole	triazole	NOUN
eurjchem-1701	25	5	rings	ring	NOUN
eurjchem-1701	25	6	have	have	AUX
eurjchem-1701	25	7	been	be	AUX
eurjchem-1701	25	8	incorporated	incorporate	VERB
eurjchem-1701	25	9	into	into	ADP
eurjchem-1701	25	10	a	a	DET
eurjchem-1701	25	11	wide	wide	ADJ
eurjchem-1701	25	12	variety	variety	NOUN
eurjchem-1701	25	13	of	of	ADP
eurjchem-1701	25	14	therapeutically	therapeutically	ADV
eurjchem-1701	25	15	interesting	interesting	ADJ
eurjchem-1701	25	16	drug	drug	NOUN
eurjchem-1701	25	17	candidates	candidate	NOUN
eurjchem-1701	25	18	including	include	VERB
eurjchem-1701	25	19	antiviral	antiviral	ADJ
eurjchem-1701	25	20	(	(	PUNCT
eurjchem-1701	25	21	ribavarin	ribavarin	NOUN
eurjchem-1701	25	22	)	)	PUNCT
eurjchem-1701	25	23	,	,	PUNCT
eurjchem-1701	25	24	antimigraine	antimigraine	NOUN
eurjchem-1701	25	25	(	(	PUNCT
eurjchem-1701	25	26	rizatriptan	rizatriptan	PROPN
eurjchem-1701	25	27	)	)	PUNCT
eurjchem-1701	25	28	(	(	PUNCT
eurjchem-1701	25	29	figure	figure	NOUN
eurjchem-1701	25	30	1	1	NUM
eurjchem-1701	25	31	)	)	PUNCT
eurjchem-1701	26	1	[	[	X
eurjchem-1701	26	2	8	8	NUM
eurjchem-1701	26	3	-	-	SYM
eurjchem-1701	26	4	10	10	NUM
eurjchem-1701	26	5	]	]	PUNCT
eurjchem-1701	26	6	,	,	PUNCT
eurjchem-1701	26	7	cns	cns	PROPN
eurjchem-1701	26	8	stimulants	stimulant	NOUN
eurjchem-1701	26	9	sedatives	sedative	NOUN
eurjchem-1701	26	10	and	and	CCONJ
eurjchem-1701	26	11	antianxiety	antianxiety	NOUN
eurjchem-1701	26	12	[	[	X
eurjchem-1701	26	13	11,12	11,12	NUM
eurjchem-1701	26	14	]	]	X
eurjchem-1701	26	15	agents	agent	NOUN
eurjchem-1701	26	16	.	.	PUNCT
eurjchem-1701	27	1	compounds	compound	NOUN
eurjchem-1701	27	2	connecting	connect	VERB
eurjchem-1701	27	3	to	to	ADP
eurjchem-1701	27	4	1,2,4triazole	1,2,4triazole	NUM
eurjchem-1701	27	5	moiety	moiety	NOUN
eurjchem-1701	27	6	are	be	AUX
eurjchem-1701	27	7	famous	famous	ADJ
eurjchem-1701	27	8	for	for	ADP
eurjchem-1701	27	9	powerful	powerful	ADJ
eurjchem-1701	27	10	antitumorial	antitumorial	NOUN
eurjchem-1701	27	11	and	and	CCONJ
eurjchem-1701	27	12	antihiv	antihiv	PROPN
eurjchem-1701	27	13	agents	agent	NOUN
eurjchem-1701	28	1	[	[	X
eurjchem-1701	28	2	13	13	NUM
eurjchem-1701	28	3	-	-	SYM
eurjchem-1701	28	4	15	15	NUM
eurjchem-1701	28	5	]	]	PUNCT
eurjchem-1701	28	6	.	.	PUNCT
eurjchem-1701	29	1	the	the	DET
eurjchem-1701	29	2	synthetic	synthetic	ADJ
eurjchem-1701	29	3	nucleoside	nucleoside	NOUN
eurjchem-1701	29	4	ribavirin	ribavirin	NOUN
eurjchem-1701	29	5	involving	involve	VERB
eurjchem-1701	29	6	a	a	DET
eurjchem-1701	29	7	1,2,4	1,2,4	NUM
eurjchem-1701	29	8	-	-	PUNCT
eurjchem-1701	29	9	triazole	triazole	NOUN
eurjchem-1701	29	10	nuclus	nuclus	NOUN
eurjchem-1701	29	11	has	have	AUX
eurjchem-1701	29	12	become	become	VERB
eurjchem-1701	29	13	an	an	DET
eurjchem-1701	29	14	outstanding	outstanding	ADJ
eurjchem-1701	29	15	drug	drug	NOUN
eurjchem-1701	29	16	when	when	SCONJ
eurjchem-1701	29	17	combined	combine	VERB
eurjchem-1701	29	18	with	with	ADP
eurjchem-1701	29	19	the	the	DET
eurjchem-1701	29	20	pegylated	pegylated	ADJ
eurjchem-1701	29	21	interferon	interferon	NOUN
eurjchem-1701	29	22	-	-	PUNCT
eurjchem-1701	29	23	α	α	NOUN
eurjchem-1701	29	24	,	,	PUNCT
eurjchem-1701	29	25	for	for	ADP
eurjchem-1701	29	26	the	the	DET
eurjchem-1701	29	27	treatment	treatment	NOUN
eurjchem-1701	29	28	of	of	ADP
eurjchem-1701	29	29	hepatitis	hepatitis	PROPN
eurjchem-1701	29	30	c	c	PROPN
eurjchem-1701	29	31	virus	virus	NOUN
eurjchem-1701	29	32	infections	infection	NOUN
eurjchem-1701	29	33	[	[	X
eurjchem-1701	29	34	16	16	NUM
eurjchem-1701	29	35	]	]	PUNCT
eurjchem-1701	29	36	.	.	PUNCT
eurjchem-1701	30	1	we	we	PRON
eurjchem-1701	30	2	have	have	AUX
eurjchem-1701	30	3	published	publish	VERB
eurjchem-1701	30	4	some	some	DET
eurjchem-1701	30	5	papers	paper	NOUN
eurjchem-1701	30	6	containing	contain	VERB
eurjchem-1701	30	7	the	the	DET
eurjchem-1701	30	8	synthesis	synthesis	NOUN
eurjchem-1701	30	9	of	of	ADP
eurjchem-1701	30	10	some	some	DET
eurjchem-1701	30	11	new	new	ADJ
eurjchem-1701	30	12	1,2,4	1,2,4	NUM
eurjchem-1701	30	13	-	-	PUNCT
eurjchem-1701	30	14	triazoles	triazole	NOUN
eurjchem-1701	30	15	attached	attach	VERB
eurjchem-1701	30	16	with	with	ADP
eurjchem-1701	30	17	several	several	ADJ
eurjchem-1701	30	18	alkyl	alkyl	NOUN
eurjchem-1701	30	19	as	as	ADV
eurjchem-1701	30	20	well	well	ADV
eurjchem-1701	30	21	as	as	ADP
eurjchem-1701	30	22	their	their	PRON
eurjchem-1701	30	23	activities	activity	NOUN
eurjchem-1701	30	24	towards	towards	ADP
eurjchem-1701	30	25	various	various	ADJ
eurjchem-1701	30	26	cyclizing	cyclize	VERB
eurjchem-1701	30	27	agents	agent	NOUN
eurjchem-1701	30	28	[	[	X
eurjchem-1701	30	29	17	17	NUM
eurjchem-1701	30	30	-	-	SYM
eurjchem-1701	30	31	20	20	NUM
eurjchem-1701	30	32	]	]	PUNCT
eurjchem-1701	30	33	.	.	PUNCT
eurjchem-1701	31	1	as	as	ADP
eurjchem-1701	31	2	a	a	DET
eurjchem-1701	31	3	result	result	NOUN
eurjchem-1701	31	4	,	,	PUNCT
eurjchem-1701	31	5	our	our	PRON
eurjchem-1701	31	6	interest	interest	NOUN
eurjchem-1701	31	7	has	have	AUX
eurjchem-1701	31	8	been	be	AUX
eurjchem-1701	31	9	recently	recently	ADV
eurjchem-1701	31	10	directed	direct	VERB
eurjchem-1701	31	11	towards	towards	ADP
eurjchem-1701	31	12	the	the	DET
eurjchem-1701	31	13	synthesis	synthesis	NOUN
eurjchem-1701	31	14	of	of	ADP
eurjchem-1701	31	15	some	some	DET
eurjchem-1701	31	16	novel	novel	ADJ
eurjchem-1701	31	17	azoles	azole	NOUN
eurjchem-1701	31	18	and	and	CCONJ
eurjchem-1701	31	19	azines	azine	NOUN
eurjchem-1701	31	20	of	of	ADP
eurjchem-1701	31	21	expected	expect	VERB
eurjchem-1701	31	22	antitumor	antitumor	NOUN
eurjchem-1701	31	23	activity	activity	NOUN
eurjchem-1701	31	24	[	[	X
eurjchem-1701	31	25	21,22	21,22	NOUN
eurjchem-1701	31	26	]	]	X
eurjchem-1701	31	27	.	.	PUNCT
eurjchem-1701	32	1	2	2	X
eurjchem-1701	32	2	.	.	X
eurjchem-1701	32	3	experimental	experimental	ADJ
eurjchem-1701	32	4	2.1	2.1	NUM
eurjchem-1701	32	5	.	.	PUNCT
eurjchem-1701	32	6	materials	material	NOUN
eurjchem-1701	32	7	all	all	DET
eurjchem-1701	32	8	experiments	experiment	NOUN
eurjchem-1701	32	9	were	be	AUX
eurjchem-1701	32	10	performed	perform	VERB
eurjchem-1701	32	11	using	use	VERB
eurjchem-1701	32	12	drying	dry	VERB
eurjchem-1701	32	13	solvents	solvent	NOUN
eurjchem-1701	32	14	.	.	PUNCT
eurjchem-1701	33	1	thin	thin	ADJ
eurjchem-1701	33	2	-	-	PUNCT
eurjchem-1701	33	3	layer	layer	NOUN
eurjchem-1701	33	4	chromatography	chromatography	NOUN
eurjchem-1701	33	5	(	(	PUNCT
eurjchem-1701	33	6	tlc	tlc	NOUN
eurjchem-1701	33	7	)	)	PUNCT
eurjchem-1701	33	8	was	be	AUX
eurjchem-1701	33	9	performed	perform	VERB
eurjchem-1701	33	10	on	on	ADP
eurjchem-1701	33	11	a	a	DET
eurjchem-1701	33	12	merck	merck	NOUN
eurjchem-1701	33	13	silica	silica	NOUN
eurjchem-1701	33	14	gel	gel	NOUN
eurjchem-1701	33	15	60f254	60f254	NOUN
eurjchem-1701	33	16	with	with	ADP
eurjchem-1701	33	17	detection	detection	NOUN
eurjchem-1701	33	18	by	by	ADP
eurjchem-1701	33	19	uv	uv	NOUN
eurjchem-1701	33	20	light	light	NOUN
eurjchem-1701	33	21	.	.	PUNCT
eurjchem-1701	34	1	products	product	NOUN
eurjchem-1701	34	2	were	be	AUX
eurjchem-1701	34	3	purified	purify	VERB
eurjchem-1701	34	4	by	by	ADP
eurjchem-1701	34	5	crystallization	crystallization	NOUN
eurjchem-1701	34	6	.	.	PUNCT
eurjchem-1701	35	1	2.2	2.2	NUM
eurjchem-1701	35	2	.	.	PUNCT
eurjchem-1701	35	3	instrumentation	instrumentation	NOUN
eurjchem-1701	35	4	we	we	PRON
eurjchem-1701	35	5	measured	measure	VERB
eurjchem-1701	35	6	the	the	DET
eurjchem-1701	35	7	melting	melting	NOUN
eurjchem-1701	35	8	points	point	NOUN
eurjchem-1701	35	9	that	that	PRON
eurjchem-1701	35	10	are	be	AUX
eurjchem-1701	35	11	uncorrected	uncorrecte	VERB
eurjchem-1701	35	12	by	by	ADP
eurjchem-1701	35	13	an	an	DET
eurjchem-1701	35	14	electro	electro	ADJ
eurjchem-1701	35	15	thermal	thermal	ADJ
eurjchem-1701	35	16	ia	ia	PROPN
eurjchem-1701	35	17	9100	9100	NUM
eurjchem-1701	35	18	apparatus	apparatus	NOUN
eurjchem-1701	35	19	with	with	ADP
eurjchem-1701	35	20	open	open	ADJ
eurjchem-1701	35	21	capillary	capillary	ADJ
eurjchem-1701	35	22	tubes	tube	NOUN
eurjchem-1701	35	23	.	.	PUNCT
eurjchem-1701	36	1	the	the	DET
eurjchem-1701	36	2	ir	ir	PROPN
eurjchem-1701	36	3	spectra	spectra	PROPN
eurjchem-1701	36	4	(	(	PUNCT
eurjchem-1701	36	5	kbr	kbr	PROPN
eurjchem-1701	36	6	disc	disc	NOUN
eurjchem-1701	36	7	)	)	PUNCT
eurjchem-1701	36	8	were	be	AUX
eurjchem-1701	36	9	recorded	record	VERB
eurjchem-1701	36	10	on	on	ADP
eurjchem-1701	36	11	a	a	DET
eurjchem-1701	36	12	pye	pye	NOUN
eurjchem-1701	36	13	unicam	unicam	ADV
eurjchem-1701	36	14	sp-3	sp-3	NOUN
eurjchem-1701	36	15	-	-	PUNCT
eurjchem-1701	36	16	300	300	NUM
eurjchem-1701	36	17	or	or	CCONJ
eurjchem-1701	36	18	a	a	DET
eurjchem-1701	36	19	shimadzu	shimadzu	ADJ
eurjchem-1701	36	20	ftir	ftir	X
eurjchem-1701	36	21	8101	8101	NUM
eurjchem-1701	36	22	pc	pc	NOUN
eurjchem-1701	36	23	infrared	infrare	VERB
eurjchem-1701	36	24	spectrophotometer	spectrophotometer	NOUN
eurjchem-1701	36	25	.	.	PUNCT
eurjchem-1701	37	1	abstract	abstract	ADJ
eurjchem-1701	37	2	research	research	NOUN
eurjchem-1701	37	3	article	article	NOUN
eurjchem-1701	37	4	keywords	keyword	VERB
eurjchem-1701	37	5	european	european	PROPN
eurjchem-1701	37	6	journal	journal	PROPN
eurjchem-1701	37	7	of	of	ADP
eurjchem-1701	37	8	chemistry	chemistry	NOUN
eurjchem-1701	37	9	issn	issn	VERB
eurjchem-1701	37	10	2153	2153	NUM
eurjchem-1701	37	11	-	-	SYM
eurjchem-1701	37	12	2249	2249	NUM
eurjchem-1701	37	13	(	(	PUNCT
eurjchem-1701	37	14	print	print	NOUN
eurjchem-1701	37	15	)	)	PUNCT
eurjchem-1701	37	16	/	/	PUNCT
eurjchem-1701	37	17	issn	issn	PROPN
eurjchem-1701	37	18	2153	2153	NUM
eurjchem-1701	37	19	-	-	SYM
eurjchem-1701	37	20	2257	2257	NUM
eurjchem-1701	37	21	(	(	PUNCT
eurjchem-1701	37	22	online	online	ADJ
eurjchem-1701	37	23	)	)	PUNCT
eurjchem-1701	37	24	–	–	PUNCT
eurjchem-1701	38	1	copyright	copyright	NOUN
eurjchem-1701	38	2	©	©	PROPN
eurjchem-1701	38	3	2018	2018	NUM
eurjchem-1701	38	4	the	the	DET
eurjchem-1701	38	5	authors	author	NOUN
eurjchem-1701	38	6	–	–	PUNCT
eurjchem-1701	38	7	atlanta	atlanta	PROPN
eurjchem-1701	38	8	publishing	publishing	PROPN
eurjchem-1701	38	9	house	house	PROPN
eurjchem-1701	38	10	llc	llc	PROPN
eurjchem-1701	38	11	–	–	PUNCT
eurjchem-1701	38	12	printed	print	VERB
eurjchem-1701	38	13	in	in	ADP
eurjchem-1701	38	14	the	the	DET
eurjchem-1701	38	15	usa	usa	PROPN
eurjchem-1701	38	16	.	.	PUNCT
eurjchem-1701	39	1	this	this	DET
eurjchem-1701	39	2	work	work	NOUN
eurjchem-1701	39	3	is	be	AUX
eurjchem-1701	39	4	published	publish	VERB
eurjchem-1701	39	5	and	and	CCONJ
eurjchem-1701	39	6	licensed	license	VERB
eurjchem-1701	39	7	by	by	ADP
eurjchem-1701	39	8	atlanta	atlanta	PROPN
eurjchem-1701	39	9	publishing	publishing	PROPN
eurjchem-1701	39	10	house	house	PROPN
eurjchem-1701	39	11	llc	llc	PROPN
eurjchem-1701	39	12	–	–	PUNCT
eurjchem-1701	39	13	cc	cc	PROPN
eurjchem-1701	39	14	by	by	ADP
eurjchem-1701	39	15	nc	nc	PROPN
eurjchem-1701	39	16	–	–	PUNCT
eurjchem-1701	39	17	some	some	DET
eurjchem-1701	39	18	rights	right	NOUN
eurjchem-1701	39	19	reserved	reserve	VERB
eurjchem-1701	39	20	.	.	PUNCT
eurjchem-1701	40	1	http://dx.doi.org/10.5155/eurjchem.9.2.99-106.1701	http://dx.doi.org/10.5155/eurjchem.9.2.99-106.1701	PROPN
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eurjchem-1701	40	3	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.9.2.99-106.1701&domain=pdf&date_stamp=2018-06-30	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.9.2.99-106.1701&domain=pdf&date_stamp=2018-06-30	PROPN
eurjchem-1701	40	4	http://www.eurjchem.com/	http://www.eurjchem.com/	PROPN
eurjchem-1701	40	5	http://dx.doi.org/10.5155/eurjchem.9.2.99-106.1701	http://dx.doi.org/10.5155/eurjchem.9.2.99-106.1701	PROPN
eurjchem-1701	40	6	mailto:rhaggan99@hotmail.com	mailto:rhaggan99@hotmail.com	PROPN
eurjchem-1701	40	7	mailto:m_gomaa59@yahoo.com	mailto:m_gomaa59@yahoo.com	PROPN
eurjchem-1701	41	1	mailto:mohasherif@yahoo.com	mailto:mohasherif@yahoo.com	PROPN
eurjchem-1701	41	2	mailto:mgalahom@yahoo.com	mailto:mgalahom@yahoo.com	PROPN
eurjchem-1701	41	3	mailto:rhaggan99@hotmail.com	mailto:rhaggan99@hotmail.com	PROPN
eurjchem-1701	41	4	http://www.eurjchem.com/	http://www.eurjchem.com/	PROPN
eurjchem-1701	41	5	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.9.2.99-106.1701&domain=pdf&date_stamp=2018-06-30	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.9.2.99-106.1701&domain=pdf&date_stamp=2018-06-30	PROPN
eurjchem-1701	41	6	�	�	PROPN
eurjchem-1701	41	7	100	100	NUM
eurjchem-1701	41	8	haggam	haggam	NOUN
eurjchem-1701	41	9	et	et	PROPN
eurjchem-1701	41	10	al	al	PROPN
eurjchem-1701	41	11	.	.	PUNCT
eurjchem-1701	41	12	/	/	SYM
eurjchem-1701	41	13	european	european	PROPN
eurjchem-1701	41	14	journal	journal	PROPN
eurjchem-1701	41	15	of	of	ADP
eurjchem-1701	41	16	chemistry	chemistry	NOUN
eurjchem-1701	41	17	9	9	NUM
eurjchem-1701	41	18	(	(	PUNCT
eurjchem-1701	41	19	2	2	NUM
eurjchem-1701	41	20	)	)	PUNCT
eurjchem-1701	41	21	(	(	PUNCT
eurjchem-1701	41	22	2018	2018	NUM
eurjchem-1701	41	23	)	)	PUNCT
eurjchem-1701	41	24	99	99	NUM
eurjchem-1701	41	25	-	-	SYM
eurjchem-1701	41	26	106	106	NUM
eurjchem-1701	41	27	n	n	CCONJ
eurjchem-1701	41	28	ho	ho	ADJ
eurjchem-1701	42	1	oh	oh	INTJ
eurjchem-1701	42	2	ho	ho	PROPN
eurjchem-1701	42	3	n	n	CCONJ
eurjchem-1701	42	4	n	n	NOUN
eurjchem-1701	42	5	o	o	NOUN
eurjchem-1701	42	6	nh2	nh2	PROPN
eurjchem-1701	42	7	rizatriptanribavarin	rizatriptanribavarin	NOUN
eurjchem-1701	42	8	n	n	CCONJ
eurjchem-1701	42	9	n	n	CCONJ
eurjchem-1701	42	10	n	n	CCONJ
eurjchem-1701	42	11	n	n	NOUN
eurjchem-1701	42	12	h	h	NOUN
eurjchem-1701	42	13	n	n	PRON
eurjchem-1701	42	14	figure	figure	VERB
eurjchem-1701	42	15	1	1	NUM
eurjchem-1701	42	16	.	.	PUNCT
eurjchem-1701	43	1	structure	structure	NOUN
eurjchem-1701	43	2	of	of	ADP
eurjchem-1701	43	3	ribavirin	ribavirin	NOUN
eurjchem-1701	43	4	and	and	CCONJ
eurjchem-1701	43	5	rizatriptan	rizatriptan	NOUN
eurjchem-1701	43	6	.	.	PUNCT
eurjchem-1701	44	1	the	the	DET
eurjchem-1701	44	2	1hand	1hand	NUM
eurjchem-1701	44	3	13c	13c	NOUN
eurjchem-1701	44	4	-	-	ADJ
eurjchem-1701	44	5	nmr	nmr	ADJ
eurjchem-1701	44	6	spectra	spectra	NOUN
eurjchem-1701	44	7	were	be	AUX
eurjchem-1701	44	8	recorded	record	VERB
eurjchem-1701	44	9	at	at	ADP
eurjchem-1701	44	10	a	a	DET
eurjchem-1701	44	11	varian	varian	PROPN
eurjchem-1701	44	12	mercury	mercury	PROPN
eurjchem-1701	44	13	vx-300	vx-300	PROPN
eurjchem-1701	44	14	nmr	nmr	NOUN
eurjchem-1701	44	15	(	(	PUNCT
eurjchem-1701	44	16	1h	1h	NUM
eurjchem-1701	44	17	,	,	PUNCT
eurjchem-1701	44	18	300	300	NUM
eurjchem-1701	44	19	mhz	mhz	NOUN
eurjchem-1701	44	20	,	,	PUNCT
eurjchem-1701	44	21	13c	13c	NOUN
eurjchem-1701	44	22	,	,	PUNCT
eurjchem-1701	44	23	75.4	75.4	NUM
eurjchem-1701	44	24	mhz	mhz	NOUN
eurjchem-1701	44	25	)	)	PUNCT
eurjchem-1701	44	26	spectrometer	spectrometer	NOUN
eurjchem-1701	44	27	using	use	VERB
eurjchem-1701	44	28	dmso	dmso	NOUN
eurjchem-1701	44	29	-	-	PUNCT
eurjchem-1701	44	30	d6	d6	NOUN
eurjchem-1701	44	31	as	as	ADP
eurjchem-1701	44	32	a	a	DET
eurjchem-1701	44	33	solvent	solvent	NOUN
eurjchem-1701	44	34	.	.	PUNCT
eurjchem-1701	45	1	all	all	DET
eurjchem-1701	45	2	chemical	chemical	ADJ
eurjchem-1701	45	3	shifts	shift	NOUN
eurjchem-1701	45	4	were	be	AUX
eurjchem-1701	45	5	expressed	express	VERB
eurjchem-1701	45	6	on	on	ADP
eurjchem-1701	45	7	the	the	DET
eurjchem-1701	45	8	δ	δ	PROPN
eurjchem-1701	45	9	(	(	PUNCT
eurjchem-1701	45	10	ppm	ppm	NOUN
eurjchem-1701	45	11	)	)	PUNCT
eurjchem-1701	45	12	scale	scale	NOUN
eurjchem-1701	45	13	using	use	VERB
eurjchem-1701	45	14	tms	tms	PROPN
eurjchem-1701	45	15	as	as	ADP
eurjchem-1701	45	16	an	an	DET
eurjchem-1701	45	17	internal	internal	ADJ
eurjchem-1701	45	18	standard	standard	ADJ
eurjchem-1701	45	19	reference	reference	NOUN
eurjchem-1701	45	20	.	.	PUNCT
eurjchem-1701	46	1	the	the	DET
eurjchem-1701	46	2	coupling	couple	VERB
eurjchem-1701	46	3	constant	constant	ADJ
eurjchem-1701	46	4	(	(	PUNCT
eurjchem-1701	46	5	ј	ј	X
eurjchem-1701	46	6	)	)	PUNCT
eurjchem-1701	46	7	values	value	NOUN
eurjchem-1701	46	8	are	be	AUX
eurjchem-1701	46	9	given	give	VERB
eurjchem-1701	46	10	in	in	ADP
eurjchem-1701	46	11	hz	hz	PROPN
eurjchem-1701	46	12	.	.	PROPN
eurjchem-1701	46	13	mass	mass	PROPN
eurjchem-1701	46	14	spectrometry	spectrometry	NOUN
eurjchem-1701	46	15	and	and	CCONJ
eurjchem-1701	46	16	analytical	analytical	ADJ
eurjchem-1701	46	17	data	datum	NOUN
eurjchem-1701	46	18	were	be	AUX
eurjchem-1701	46	19	obtained	obtain	VERB
eurjchem-1701	46	20	from	from	ADP
eurjchem-1701	46	21	the	the	DET
eurjchem-1701	46	22	microanalysis	microanalysis	ADJ
eurjchem-1701	46	23	center	center	NOUN
eurjchem-1701	46	24	at	at	ADP
eurjchem-1701	46	25	cairo	cairo	PROPN
eurjchem-1701	46	26	university	university	PROPN
eurjchem-1701	46	27	,	,	PUNCT
eurjchem-1701	46	28	giza	giza	PROPN
eurjchem-1701	46	29	,	,	PUNCT
eurjchem-1701	46	30	egypt	egypt	PROPN
eurjchem-1701	46	31	.	.	PUNCT
eurjchem-1701	47	1	2.3	2.3	NUM
eurjchem-1701	47	2	.	.	PUNCT
eurjchem-1701	48	1	synthesis	synthesis	NOUN
eurjchem-1701	48	2	2.3.1	2.3.1	NUM
eurjchem-1701	48	3	.	.	PUNCT
eurjchem-1701	48	4	synthesis	synthesis	NOUN
eurjchem-1701	48	5	of	of	ADP
eurjchem-1701	48	6	n-((thiophene-2	n-((thiophene-2	PROPN
eurjchem-1701	48	7	-	-	PUNCT
eurjchem-1701	48	8	carbonyl)carbamothio	carbonyl)carbamothio	ADJ
eurjchem-1701	48	9	yl)hydrazinecarboxamide	yl)hydrazinecarboxamide	ADJ
eurjchem-1701	48	10	hydrochloride	hydrochloride	NOUN
eurjchem-1701	48	11	(	(	PUNCT
eurjchem-1701	48	12	2	2	NUM
eurjchem-1701	48	13	)	)	PUNCT
eurjchem-1701	48	14	a	a	DET
eurjchem-1701	48	15	mixture	mixture	NOUN
eurjchem-1701	48	16	of	of	ADP
eurjchem-1701	48	17	thiophene-2	thiophene-2	NOUN
eurjchem-1701	48	18	-	-	PUNCT
eurjchem-1701	48	19	carbonylisothiocyanate	carbonylisothiocyanate	NOUN
eurjchem-1701	48	20	(	(	PUNCT
eurjchem-1701	48	21	1	1	NUM
eurjchem-1701	48	22	)	)	PUNCT
eurjchem-1701	48	23	(	(	PUNCT
eurjchem-1701	48	24	3.40	3.40	NUM
eurjchem-1701	48	25	mol	mol	NOUN
eurjchem-1701	48	26	)	)	PUNCT
eurjchem-1701	48	27	and	and	CCONJ
eurjchem-1701	48	28	semicarbazide	semicarbazide	ADJ
eurjchem-1701	48	29	hydrochloride	hydrochloride	NOUN
eurjchem-1701	48	30	(	(	PUNCT
eurjchem-1701	48	31	3.40	3.40	NUM
eurjchem-1701	48	32	mol	mol	NOUN
eurjchem-1701	48	33	)	)	PUNCT
eurjchem-1701	48	34	in	in	ADP
eurjchem-1701	48	35	dioxane	dioxane	NOUN
eurjchem-1701	48	36	:	:	PUNCT
eurjchem-1701	48	37	water	water	NOUN
eurjchem-1701	48	38	(	(	PUNCT
eurjchem-1701	48	39	1:1	1:1	NUM
eurjchem-1701	48	40	,	,	PUNCT
eurjchem-1701	48	41	v	v	NOUN
eurjchem-1701	48	42	:	:	SYM
eurjchem-1701	48	43	v	v	NOUN
eurjchem-1701	48	44	)	)	PUNCT
eurjchem-1701	48	45	(	(	PUNCT
eurjchem-1701	48	46	50	50	NUM
eurjchem-1701	48	47	ml	ml	NOUN
eurjchem-1701	48	48	)	)	PUNCT
eurjchem-1701	48	49	was	be	AUX
eurjchem-1701	48	50	stirred	stir	VERB
eurjchem-1701	48	51	at	at	ADP
eurjchem-1701	48	52	room	room	NOUN
eurjchem-1701	48	53	temperature	temperature	NOUN
eurjchem-1701	48	54	for	for	ADP
eurjchem-1701	48	55	1	1	NUM
eurjchem-1701	48	56	h.	h.	NOUN
eurjchem-1701	48	57	the	the	DET
eurjchem-1701	48	58	reaction	reaction	NOUN
eurjchem-1701	48	59	mixture	mixture	NOUN
eurjchem-1701	48	60	was	be	AUX
eurjchem-1701	48	61	poured	pour	VERB
eurjchem-1701	48	62	into	into	ADP
eurjchem-1701	48	63	cold	cold	ADJ
eurjchem-1701	48	64	water	water	NOUN
eurjchem-1701	48	65	.	.	PUNCT
eurjchem-1701	49	1	the	the	DET
eurjchem-1701	49	2	formed	form	VERB
eurjchem-1701	49	3	precipitate	precipitate	NOUN
eurjchem-1701	49	4	was	be	AUX
eurjchem-1701	49	5	filtered	filter	VERB
eurjchem-1701	49	6	off	off	ADP
eurjchem-1701	49	7	,	,	PUNCT
eurjchem-1701	49	8	washed	wash	VERB
eurjchem-1701	49	9	with	with	ADP
eurjchem-1701	49	10	cold	cold	ADJ
eurjchem-1701	49	11	water	water	NOUN
eurjchem-1701	49	12	,	,	PUNCT
eurjchem-1701	49	13	dried	dry	VERB
eurjchem-1701	49	14	and	and	CCONJ
eurjchem-1701	49	15	crystallized	crystallize	VERB
eurjchem-1701	49	16	from	from	ADP
eurjchem-1701	49	17	ethanol	ethanol	NOUN
eurjchem-1701	49	18	to	to	PART
eurjchem-1701	49	19	give	give	VERB
eurjchem-1701	49	20	compound	compound	NOUN
eurjchem-1701	49	21	2	2	NUM
eurjchem-1701	49	22	(	(	PUNCT
eurjchem-1701	49	23	scheme	scheme	NOUN
eurjchem-1701	49	24	1	1	NUM
eurjchem-1701	49	25	)	)	PUNCT
eurjchem-1701	49	26	.	.	PUNCT
eurjchem-1701	50	1	color	color	NOUN
eurjchem-1701	50	2	:	:	PUNCT
eurjchem-1701	50	3	white	white	ADJ
eurjchem-1701	50	4	.	.	PUNCT
eurjchem-1701	51	1	yield	yield	NOUN
eurjchem-1701	51	2	:	:	PUNCT
eurjchem-1701	51	3	33	33	NUM
eurjchem-1701	51	4	%	%	NOUN
eurjchem-1701	51	5	.	.	PUNCT
eurjchem-1701	52	1	m.p	m.p	PROPN
eurjchem-1701	52	2	.	.	PROPN
eurjchem-1701	52	3	:	:	PUNCT
eurjchem-1701	53	1	210	210	NUM
eurjchem-1701	53	2	-	-	SYM
eurjchem-1701	53	3	211	211	NUM
eurjchem-1701	53	4	°	°	NOUN
eurjchem-1701	53	5	c	c	NOUN
eurjchem-1701	53	6	.	.	PUNCT
eurjchem-1701	53	7	ft	ft	PROPN
eurjchem-1701	53	8	-	-	PUNCT
eurjchem-1701	53	9	ir	ir	PROPN
eurjchem-1701	53	10	(	(	PUNCT
eurjchem-1701	53	11	kbr	kbr	PROPN
eurjchem-1701	53	12	,	,	PUNCT
eurjchem-1701	53	13	ν	ν	PROPN
eurjchem-1701	53	14	,	,	PUNCT
eurjchem-1701	53	15	cm-1	cm-1	NUM
eurjchem-1701	53	16	):	):	PUNCT
eurjchem-1701	53	17	3433	3433	NUM
eurjchem-1701	53	18	,	,	PUNCT
eurjchem-1701	53	19	3317	3317	NUM
eurjchem-1701	53	20	(	(	PUNCT
eurjchem-1701	53	21	nh2	nh2	PROPN
eurjchem-1701	53	22	)	)	PUNCT
eurjchem-1701	53	23	,	,	PUNCT
eurjchem-1701	53	24	3156	3156	NUM
eurjchem-1701	53	25	(	(	PUNCT
eurjchem-1701	53	26	nh	nh	NOUN
eurjchem-1701	53	27	)	)	PUNCT
eurjchem-1701	53	28	,	,	PUNCT
eurjchem-1701	53	29	3207	3207	NUM
eurjchem-1701	53	30	,	,	PUNCT
eurjchem-1701	53	31	1671	1671	NUM
eurjchem-1701	53	32	(	(	PUNCT
eurjchem-1701	53	33	c	c	NOUN
eurjchem-1701	53	34	=	=	NOUN
eurjchem-1701	53	35	o	o	NOUN
eurjchem-1701	53	36	)	)	PUNCT
eurjchem-1701	53	37	,	,	PUNCT
eurjchem-1701	53	38	1667	1667	NUM
eurjchem-1701	53	39	(	(	PUNCT
eurjchem-1701	53	40	c	c	NOUN
eurjchem-1701	53	41	=	=	SYM
eurjchem-1701	53	42	c	c	NOUN
eurjchem-1701	53	43	)	)	PUNCT
eurjchem-1701	53	44	,	,	PUNCT
eurjchem-1701	53	45	1267	1267	NUM
eurjchem-1701	53	46	(	(	PUNCT
eurjchem-1701	53	47	c	c	NOUN
eurjchem-1701	53	48	-	-	PUNCT
eurjchem-1701	53	49	o	o	NOUN
eurjchem-1701	53	50	)	)	PUNCT
eurjchem-1701	53	51	.	.	PUNCT
eurjchem-1701	53	52	1h	1h	NUM
eurjchem-1701	53	53	nmr	nmr	NOUN
eurjchem-1701	53	54	(	(	PUNCT
eurjchem-1701	53	55	300	300	NUM
eurjchem-1701	53	56	mhz	mhz	NOUN
eurjchem-1701	53	57	,	,	PUNCT
eurjchem-1701	53	58	dmso	dmso	NOUN
eurjchem-1701	53	59	-	-	NOUN
eurjchem-1701	53	60	d6	d6	NOUN
eurjchem-1701	53	61	,	,	PUNCT
eurjchem-1701	53	62	δ	δ	PROPN
eurjchem-1701	53	63	,	,	PUNCT
eurjchem-1701	53	64	ppm	ppm	NUM
eurjchem-1701	53	65	):	):	PUNCT
eurjchem-1701	53	66	7.12	7.12	NUM
eurjchem-1701	53	67	-	-	SYM
eurjchem-1701	53	68	7.86	7.86	NUM
eurjchem-1701	53	69	(	(	PUNCT
eurjchem-1701	53	70	m	m	PROPN
eurjchem-1701	53	71	,	,	PUNCT
eurjchem-1701	53	72	3h	3h	NUM
eurjchem-1701	53	73	,	,	PUNCT
eurjchem-1701	53	74	thiophene	thiophene	NOUN
eurjchem-1701	53	75	protones	protone	NOUN
eurjchem-1701	53	76	)	)	PUNCT
eurjchem-1701	53	77	,	,	PUNCT
eurjchem-1701	53	78	8.33	8.33	NUM
eurjchem-1701	53	79	(	(	PUNCT
eurjchem-1701	53	80	s	s	PROPN
eurjchem-1701	53	81	,	,	PUNCT
eurjchem-1701	53	82	1h	1h	NUM
eurjchem-1701	53	83	,	,	PUNCT
eurjchem-1701	53	84	nh	nh	PROPN
eurjchem-1701	53	85	)	)	PUNCT
eurjchem-1701	53	86	,	,	PUNCT
eurjchem-1701	53	87	8.34	8.34	NUM
eurjchem-1701	53	88	(	(	PUNCT
eurjchem-1701	53	89	s	s	PROPN
eurjchem-1701	53	90	,	,	PUNCT
eurjchem-1701	53	91	1h	1h	NUM
eurjchem-1701	53	92	,	,	PUNCT
eurjchem-1701	53	93	nh	nh	PROPN
eurjchem-1701	53	94	)	)	PUNCT
eurjchem-1701	53	95	,	,	PUNCT
eurjchem-1701	53	96	8.99	8.99	NUM
eurjchem-1701	53	97	(	(	PUNCT
eurjchem-1701	53	98	s	s	PROPN
eurjchem-1701	53	99	,	,	PUNCT
eurjchem-1701	53	100	1h	1h	NUM
eurjchem-1701	53	101	,	,	PUNCT
eurjchem-1701	53	102	nh	nh	PROPN
eurjchem-1701	53	103	)	)	PUNCT
eurjchem-1701	53	104	,	,	PUNCT
eurjchem-1701	53	105	11.63	11.63	NUM
eurjchem-1701	53	106	(	(	PUNCT
eurjchem-1701	53	107	s	s	PROPN
eurjchem-1701	53	108	,	,	PUNCT
eurjchem-1701	53	109	2h	2h	NUM
eurjchem-1701	53	110	,	,	PUNCT
eurjchem-1701	53	111	nh2	nh2	PROPN
eurjchem-1701	53	112	)	)	PUNCT
eurjchem-1701	53	113	.	.	PUNCT
eurjchem-1701	54	1	13c	13c	NOUN
eurjchem-1701	54	2	nmr	nmr	NOUN
eurjchem-1701	54	3	(	(	PUNCT
eurjchem-1701	54	4	75.4	75.4	NUM
eurjchem-1701	54	5	mhz	mhz	NOUN
eurjchem-1701	54	6	,	,	PUNCT
eurjchem-1701	54	7	dmso	dmso	NOUN
eurjchem-1701	54	8	-	-	NOUN
eurjchem-1701	54	9	d6	d6	NOUN
eurjchem-1701	54	10	,	,	PUNCT
eurjchem-1701	54	11	δ	δ	PROPN
eurjchem-1701	54	12	,	,	PUNCT
eurjchem-1701	54	13	ppm	ppm	NUM
eurjchem-1701	54	14	):	):	PUNCT
eurjchem-1701	54	15	167.1	167.1	NUM
eurjchem-1701	54	16	(	(	PUNCT
eurjchem-1701	54	17	1c	1c	NOUN
eurjchem-1701	54	18	,	,	PUNCT
eurjchem-1701	54	19	ncs	ncs	NOUN
eurjchem-1701	54	20	)	)	PUNCT
eurjchem-1701	54	21	,	,	PUNCT
eurjchem-1701	54	22	165.2	165.2	NUM
eurjchem-1701	54	23	,	,	PUNCT
eurjchem-1701	54	24	164.3	164.3	NUM
eurjchem-1701	54	25	(	(	PUNCT
eurjchem-1701	54	26	2c	2c	NOUN
eurjchem-1701	54	27	,	,	PUNCT
eurjchem-1701	54	28	2c	2c	NOUN
eurjchem-1701	54	29	=	=	SYM
eurjchem-1701	54	30	o	o	NOUN
eurjchem-1701	54	31	)	)	PUNCT
eurjchem-1701	54	32	,	,	PUNCT
eurjchem-1701	54	33	129.8	129.8	NUM
eurjchem-1701	54	34	,	,	PUNCT
eurjchem-1701	54	35	128.4	128.4	NUM
eurjchem-1701	54	36	,	,	PUNCT
eurjchem-1701	54	37	128.0	128.0	NUM
eurjchem-1701	54	38	,	,	PUNCT
eurjchem-1701	54	39	127.5	127.5	NUM
eurjchem-1701	54	40	(	(	PUNCT
eurjchem-1701	54	41	ar	ar	NOUN
eurjchem-1701	54	42	-	-	NOUN
eurjchem-1701	54	43	c	c	NOUN
eurjchem-1701	54	44	)	)	PUNCT
eurjchem-1701	54	45	.	.	PUNCT
eurjchem-1701	55	1	ms	ms	NOUN
eurjchem-1701	55	2	(	(	PUNCT
eurjchem-1701	55	3	ei	ei	PROPN
eurjchem-1701	55	4	,	,	PUNCT
eurjchem-1701	55	5	m	m	PROPN
eurjchem-1701	55	6	/	/	SYM
eurjchem-1701	55	7	z	z	PROPN
eurjchem-1701	55	8	(	(	PUNCT
eurjchem-1701	55	9	%	%	NOUN
eurjchem-1701	55	10	)	)	PUNCT
eurjchem-1701	55	11	):	):	PUNCT
eurjchem-1701	55	12	280	280	NUM
eurjchem-1701	55	13	(	(	PUNCT
eurjchem-1701	55	14	m+	m+	NUM
eurjchem-1701	55	15	,	,	PUNCT
eurjchem-1701	55	16	100	100	NUM
eurjchem-1701	55	17	)	)	PUNCT
eurjchem-1701	55	18	.	.	PUNCT
eurjchem-1701	56	1	128	128	NUM
eurjchem-1701	56	2	(	(	PUNCT
eurjchem-1701	56	3	4	4	NUM
eurjchem-1701	56	4	)	)	PUNCT
eurjchem-1701	56	5	,	,	PUNCT
eurjchem-1701	56	6	110	110	NUM
eurjchem-1701	56	7	(	(	PUNCT
eurjchem-1701	56	8	100	100	NUM
eurjchem-1701	56	9	)	)	PUNCT
eurjchem-1701	56	10	,	,	PUNCT
eurjchem-1701	56	11	83	83	NUM
eurjchem-1701	56	12	(	(	PUNCT
eurjchem-1701	56	13	30	30	NUM
eurjchem-1701	56	14	)	)	PUNCT
eurjchem-1701	56	15	,	,	PUNCT
eurjchem-1701	56	16	69	69	NUM
eurjchem-1701	56	17	(	(	PUNCT
eurjchem-1701	56	18	35	35	NUM
eurjchem-1701	56	19	)	)	PUNCT
eurjchem-1701	56	20	,	,	PUNCT
eurjchem-1701	56	21	57	57	NUM
eurjchem-1701	56	22	(	(	PUNCT
eurjchem-1701	56	23	60	60	NUM
eurjchem-1701	56	24	)	)	PUNCT
eurjchem-1701	56	25	.	.	PUNCT
eurjchem-1701	57	1	2.3.2	2.3.2	NUM
eurjchem-1701	57	2	.	.	X
eurjchem-1701	57	3	synthesis	synthesis	NOUN
eurjchem-1701	57	4	of	of	ADP
eurjchem-1701	57	5	2	2	NUM
eurjchem-1701	57	6	-	-	PUNCT
eurjchem-1701	57	7	hydrazinyl-6-(thiophen-2	hydrazinyl-6-(thiophen-2	NOUN
eurjchem-1701	57	8	-	-	PUNCT
eurjchem-1701	57	9	yl)-4h-1,3,5oxadiazine-4	yl)-4h-1,3,5oxadiazine-4	NOUN
eurjchem-1701	57	10	-	-	PUNCT
eurjchem-1701	57	11	thione	thione	NOUN
eurjchem-1701	57	12	(	(	PUNCT
eurjchem-1701	57	13	3	3	NUM
eurjchem-1701	57	14	)	)	PUNCT
eurjchem-1701	57	15	a	a	DET
eurjchem-1701	57	16	mixture	mixture	NOUN
eurjchem-1701	57	17	of	of	ADP
eurjchem-1701	57	18	n-((thiophene-2	n-((thiophene-2	PROPN
eurjchem-1701	57	19	-	-	PUNCT
eurjchem-1701	57	20	carbonyl)carbamothioyl	carbonyl)carbamothioyl	ADJ
eurjchem-1701	57	21	)	)	PUNCT
eurjchem-1701	57	22	hydrazinecarboxamide	hydrazinecarboxamide	ADV
eurjchem-1701	57	23	hydrochloride	hydrochloride	NOUN
eurjchem-1701	57	24	(	(	PUNCT
eurjchem-1701	57	25	2	2	NUM
eurjchem-1701	57	26	)	)	PUNCT
eurjchem-1701	57	27	(	(	PUNCT
eurjchem-1701	57	28	1.70	1.70	NUM
eurjchem-1701	57	29	mol	mol	NOUN
eurjchem-1701	57	30	)	)	PUNCT
eurjchem-1701	57	31	and	and	CCONJ
eurjchem-1701	57	32	sodium	sodium	NOUN
eurjchem-1701	57	33	ethoxide	ethoxide	NOUN
eurjchem-1701	57	34	(	(	PUNCT
eurjchem-1701	57	35	1.70	1.70	NUM
eurjchem-1701	57	36	mol	mol	NOUN
eurjchem-1701	57	37	)	)	PUNCT
eurjchem-1701	57	38	in	in	ADP
eurjchem-1701	57	39	ethanol	ethanol	NOUN
eurjchem-1701	57	40	(	(	PUNCT
eurjchem-1701	57	41	20	20	NUM
eurjchem-1701	57	42	ml	ml	NOUN
eurjchem-1701	57	43	)	)	PUNCT
eurjchem-1701	57	44	was	be	AUX
eurjchem-1701	57	45	heated	heat	VERB
eurjchem-1701	57	46	under	under	ADP
eurjchem-1701	57	47	reflux	reflux	NOUN
eurjchem-1701	57	48	for	for	ADP
eurjchem-1701	57	49	2	2	NUM
eurjchem-1701	57	50	h.	h.	NOUN
eurjchem-1701	57	51	the	the	DET
eurjchem-1701	57	52	reaction	reaction	NOUN
eurjchem-1701	57	53	mixture	mixture	NOUN
eurjchem-1701	57	54	was	be	AUX
eurjchem-1701	57	55	neutralized	neutralize	VERB
eurjchem-1701	57	56	by	by	ADP
eurjchem-1701	57	57	10	10	NUM
eurjchem-1701	57	58	%	%	NOUN
eurjchem-1701	57	59	hcl	hcl	PROPN
eurjchem-1701	57	60	.	.	PUNCT
eurjchem-1701	58	1	the	the	DET
eurjchem-1701	58	2	formed	form	VERB
eurjchem-1701	58	3	precipitate	precipitate	NOUN
eurjchem-1701	58	4	was	be	AUX
eurjchem-1701	58	5	filtered	filter	VERB
eurjchem-1701	58	6	off	off	ADP
eurjchem-1701	58	7	,	,	PUNCT
eurjchem-1701	58	8	dried	dry	VERB
eurjchem-1701	58	9	and	and	CCONJ
eurjchem-1701	58	10	crystallized	crystallize	VERB
eurjchem-1701	58	11	from	from	ADP
eurjchem-1701	58	12	ethanol	ethanol	NOUN
eurjchem-1701	58	13	to	to	PART
eurjchem-1701	58	14	give	give	VERB
eurjchem-1701	58	15	compound	compound	NOUN
eurjchem-1701	58	16	3	3	NUM
eurjchem-1701	58	17	(	(	PUNCT
eurjchem-1701	58	18	scheme	scheme	NOUN
eurjchem-1701	58	19	1	1	NUM
eurjchem-1701	58	20	)	)	PUNCT
eurjchem-1701	58	21	.	.	PUNCT
eurjchem-1701	59	1	color	color	NOUN
eurjchem-1701	59	2	:	:	PUNCT
eurjchem-1701	59	3	white	white	ADJ
eurjchem-1701	59	4	.	.	PUNCT
eurjchem-1701	60	1	yield	yield	NOUN
eurjchem-1701	60	2	:	:	PUNCT
eurjchem-1701	60	3	89	89	NUM
eurjchem-1701	60	4	%	%	NOUN
eurjchem-1701	60	5	.	.	PUNCT
eurjchem-1701	61	1	m.p	m.p	PROPN
eurjchem-1701	61	2	.	.	PROPN
eurjchem-1701	61	3	:	:	PUNCT
eurjchem-1701	62	1	279	279	NUM
eurjchem-1701	62	2	-	-	SYM
eurjchem-1701	62	3	280	280	NUM
eurjchem-1701	62	4	°	°	NOUN
eurjchem-1701	62	5	c	c	NOUN
eurjchem-1701	62	6	.	.	PUNCT
eurjchem-1701	63	1	ft	ft	PROPN
eurjchem-1701	63	2	-	-	PUNCT
eurjchem-1701	63	3	ir	ir	PROPN
eurjchem-1701	63	4	(	(	PUNCT
eurjchem-1701	63	5	kbr	kbr	PROPN
eurjchem-1701	63	6	,	,	PUNCT
eurjchem-1701	63	7	ν	ν	PROPN
eurjchem-1701	63	8	,	,	PUNCT
eurjchem-1701	63	9	cm1	cm1	PROPN
eurjchem-1701	63	10	):	):	PUNCT
eurjchem-1701	63	11	3411	3411	NUM
eurjchem-1701	63	12	,	,	PUNCT
eurjchem-1701	63	13	3325	3325	NUM
eurjchem-1701	63	14	(	(	PUNCT
eurjchem-1701	63	15	nh2	nh2	PROPN
eurjchem-1701	63	16	,	,	PUNCT
eurjchem-1701	63	17	nh	nh	PROPN
eurjchem-1701	63	18	)	)	PUNCT
eurjchem-1701	63	19	,	,	PUNCT
eurjchem-1701	63	20	1599	1599	NUM
eurjchem-1701	63	21	(	(	PUNCT
eurjchem-1701	63	22	c	c	X
eurjchem-1701	63	23	=	=	SYM
eurjchem-1701	63	24	c	c	NOUN
eurjchem-1701	63	25	)	)	PUNCT
eurjchem-1701	63	26	,	,	PUNCT
eurjchem-1701	63	27	1235	1235	NUM
eurjchem-1701	63	28	(	(	PUNCT
eurjchem-1701	63	29	c	c	NOUN
eurjchem-1701	63	30	-	-	PUNCT
eurjchem-1701	63	31	o	o	NOUN
eurjchem-1701	63	32	)	)	PUNCT
eurjchem-1701	63	33	.	.	PUNCT
eurjchem-1701	64	1	1h	1h	NUM
eurjchem-1701	64	2	nmr	nmr	NOUN
eurjchem-1701	64	3	(	(	PUNCT
eurjchem-1701	64	4	300	300	NUM
eurjchem-1701	64	5	mhz	mhz	NOUN
eurjchem-1701	64	6	,	,	PUNCT
eurjchem-1701	64	7	dmso	dmso	NOUN
eurjchem-1701	64	8	-	-	NOUN
eurjchem-1701	64	9	d6	d6	NOUN
eurjchem-1701	64	10	,	,	PUNCT
eurjchem-1701	64	11	δ	δ	PROPN
eurjchem-1701	64	12	,	,	PUNCT
eurjchem-1701	64	13	ppm	ppm	NUM
eurjchem-1701	64	14	):	):	PUNCT
eurjchem-1701	64	15	7.75	7.75	NUM
eurjchem-1701	64	16	-	-	SYM
eurjchem-1701	64	17	7.19	7.19	NUM
eurjchem-1701	64	18	(	(	PUNCT
eurjchem-1701	64	19	m	m	PROPN
eurjchem-1701	64	20	,	,	PUNCT
eurjchem-1701	64	21	3h	3h	NUM
eurjchem-1701	64	22	,	,	PUNCT
eurjchem-1701	64	23	thiophene	thiophene	NOUN
eurjchem-1701	64	24	protons	proton	NOUN
eurjchem-1701	64	25	)	)	PUNCT
eurjchem-1701	64	26	,	,	PUNCT
eurjchem-1701	64	27	13.61	13.61	NUM
eurjchem-1701	64	28	(	(	PUNCT
eurjchem-1701	64	29	s	s	PROPN
eurjchem-1701	64	30	,	,	PUNCT
eurjchem-1701	64	31	2h	2h	NUM
eurjchem-1701	64	32	,	,	PUNCT
eurjchem-1701	64	33	d2o	d2o	NOUN
eurjchem-1701	64	34	exchangeable	exchangeable	ADJ
eurjchem-1701	64	35	,	,	PUNCT
eurjchem-1701	64	36	nh2	nh2	PROPN
eurjchem-1701	64	37	)	)	PUNCT
eurjchem-1701	64	38	,	,	PUNCT
eurjchem-1701	64	39	13.91	13.91	NUM
eurjchem-1701	64	40	(	(	PUNCT
eurjchem-1701	64	41	1h	1h	NUM
eurjchem-1701	64	42	,	,	PUNCT
eurjchem-1701	64	43	d2o	d2o	NOUN
eurjchem-1701	64	44	exchangeable	exchangeable	ADJ
eurjchem-1701	64	45	,	,	PUNCT
eurjchem-1701	64	46	s	s	PROPN
eurjchem-1701	64	47	,	,	PUNCT
eurjchem-1701	64	48	nh	nh	PROPN
eurjchem-1701	64	49	)	)	PUNCT
eurjchem-1701	64	50	.	.	PUNCT
eurjchem-1701	65	1	1h	1h	NUM
eurjchem-1701	65	2	nmr	nmr	NOUN
eurjchem-1701	65	3	(	(	PUNCT
eurjchem-1701	65	4	300	300	NUM
eurjchem-1701	65	5	mhz	mhz	NOUN
eurjchem-1701	65	6	,	,	PUNCT
eurjchem-1701	65	7	dmso	dmso	NOUN
eurjchem-1701	65	8	-	-	NOUN
eurjchem-1701	65	9	d6	d6	NOUN
eurjchem-1701	65	10	,	,	PUNCT
eurjchem-1701	65	11	δ	δ	PROPN
eurjchem-1701	65	12	,	,	PUNCT
eurjchem-1701	65	13	h	h	NOUN
eurjchem-1701	65	14	/	/	SYM
eurjchem-1701	65	15	dexchange	dexchange	NOUN
eurjchem-1701	65	16	,	,	PUNCT
eurjchem-1701	65	17	ppm	ppm	NOUN
eurjchem-1701	65	18	):	):	PUNCT
eurjchem-1701	65	19	7.75	7.75	NUM
eurjchem-1701	65	20	-	-	SYM
eurjchem-1701	65	21	7.19	7.19	NUM
eurjchem-1701	65	22	(	(	PUNCT
eurjchem-1701	65	23	m	m	PROPN
eurjchem-1701	65	24	,	,	PUNCT
eurjchem-1701	65	25	3h	3h	NUM
eurjchem-1701	65	26	,	,	PUNCT
eurjchem-1701	65	27	thiophene	thiophene	NOUN
eurjchem-1701	65	28	protons	proton	NOUN
eurjchem-1701	65	29	)	)	PUNCT
eurjchem-1701	65	30	.	.	PUNCT
eurjchem-1701	66	1	13c	13c	NOUN
eurjchem-1701	66	2	nmr	nmr	NOUN
eurjchem-1701	66	3	(	(	PUNCT
eurjchem-1701	66	4	75.4	75.4	NUM
eurjchem-1701	66	5	mhz	mhz	NOUN
eurjchem-1701	66	6	,	,	PUNCT
eurjchem-1701	66	7	dmso	dmso	NOUN
eurjchem-1701	66	8	-	-	NOUN
eurjchem-1701	66	9	d6	d6	NOUN
eurjchem-1701	66	10	,	,	PUNCT
eurjchem-1701	66	11	δ	δ	PROPN
eurjchem-1701	66	12	,	,	PUNCT
eurjchem-1701	66	13	ppm	ppm	NUM
eurjchem-1701	66	14	):	):	PUNCT
eurjchem-1701	66	15	168.1	168.1	NUM
eurjchem-1701	66	16	(	(	PUNCT
eurjchem-1701	66	17	1c	1c	NOUN
eurjchem-1701	66	18	,	,	PUNCT
eurjchem-1701	66	19	ncs	ncs	NOUN
eurjchem-1701	66	20	)	)	PUNCT
eurjchem-1701	66	21	,	,	PUNCT
eurjchem-1701	66	22	163.6	163.6	NUM
eurjchem-1701	66	23	(	(	PUNCT
eurjchem-1701	66	24	1c	1c	NUM
eurjchem-1701	66	25	,	,	PUNCT
eurjchem-1701	66	26	ocn	ocn	PROPN
eurjchem-1701	66	27	)	)	PUNCT
eurjchem-1701	66	28	,	,	PUNCT
eurjchem-1701	66	29	155.3	155.3	NUM
eurjchem-1701	66	30	(	(	PUNCT
eurjchem-1701	66	31	1c	1c	X
eurjchem-1701	66	32	,	,	PUNCT
eurjchem-1701	66	33	ncn	ncn	NOUN
eurjchem-1701	66	34	)	)	PUNCT
eurjchem-1701	66	35	,	,	PUNCT
eurjchem-1701	66	36	129.5	129.5	NUM
eurjchem-1701	66	37	,	,	PUNCT
eurjchem-1701	66	38	128.7	128.7	NUM
eurjchem-1701	66	39	,	,	PUNCT
eurjchem-1701	66	40	128.3	128.3	NUM
eurjchem-1701	66	41	,	,	PUNCT
eurjchem-1701	66	42	127.2	127.2	NUM
eurjchem-1701	66	43	(	(	PUNCT
eurjchem-1701	66	44	ar	ar	NOUN
eurjchem-1701	66	45	-	-	NOUN
eurjchem-1701	66	46	c	c	NOUN
eurjchem-1701	66	47	)	)	PUNCT
eurjchem-1701	66	48	.	.	PUNCT
eurjchem-1701	67	1	ms	ms	NOUN
eurjchem-1701	67	2	(	(	PUNCT
eurjchem-1701	67	3	ei	ei	PROPN
eurjchem-1701	67	4	,	,	PUNCT
eurjchem-1701	67	5	m	m	PROPN
eurjchem-1701	67	6	/	/	SYM
eurjchem-1701	67	7	z	z	PROPN
eurjchem-1701	67	8	(	(	PUNCT
eurjchem-1701	67	9	%	%	NOUN
eurjchem-1701	67	10	)	)	PUNCT
eurjchem-1701	67	11	):	):	PUNCT
eurjchem-1701	67	12	226	226	NUM
eurjchem-1701	67	13	(	(	PUNCT
eurjchem-1701	67	14	m+	m+	NUM
eurjchem-1701	67	15	,	,	PUNCT
eurjchem-1701	67	16	15	15	NUM
eurjchem-1701	67	17	)	)	PUNCT
eurjchem-1701	67	18	,	,	PUNCT
eurjchem-1701	67	19	183	183	NUM
eurjchem-1701	67	20	(	(	PUNCT
eurjchem-1701	67	21	100	100	NUM
eurjchem-1701	67	22	)	)	PUNCT
eurjchem-1701	67	23	,	,	PUNCT
eurjchem-1701	67	24	124	124	NUM
eurjchem-1701	67	25	(	(	PUNCT
eurjchem-1701	67	26	35	35	NUM
eurjchem-1701	67	27	)	)	PUNCT
eurjchem-1701	67	28	,	,	PUNCT
eurjchem-1701	67	29	110	110	NUM
eurjchem-1701	67	30	(	(	PUNCT
eurjchem-1701	67	31	40	40	NUM
eurjchem-1701	67	32	)	)	PUNCT
eurjchem-1701	67	33	,	,	PUNCT
eurjchem-1701	67	34	70	70	NUM
eurjchem-1701	67	35	(	(	PUNCT
eurjchem-1701	67	36	25	25	NUM
eurjchem-1701	67	37	)	)	PUNCT
eurjchem-1701	67	38	,	,	PUNCT
eurjchem-1701	67	39	69	69	NUM
eurjchem-1701	67	40	(	(	PUNCT
eurjchem-1701	67	41	30	30	NUM
eurjchem-1701	67	42	)	)	PUNCT
eurjchem-1701	67	43	.	.	PUNCT
eurjchem-1701	68	1	anal	anal	PROPN
eurjchem-1701	68	2	.	.	PUNCT
eurjchem-1701	68	3	calcd	calcd	NOUN
eurjchem-1701	68	4	.	.	PUNCT
eurjchem-1701	69	1	for	for	ADP
eurjchem-1701	69	2	c7h6n4os2	c7h6n4os2	NOUN
eurjchem-1701	69	3	:	:	PUNCT
eurjchem-1701	69	4	c	c	X
eurjchem-1701	69	5	,	,	PUNCT
eurjchem-1701	69	6	37.16	37.16	NUM
eurjchem-1701	69	7	;	;	PUNCT
eurjchem-1701	69	8	h	h	NOUN
eurjchem-1701	69	9	,	,	PUNCT
eurjchem-1701	69	10	2.67	2.67	NUM
eurjchem-1701	69	11	;	;	PUNCT
eurjchem-1701	69	12	n	n	CCONJ
eurjchem-1701	69	13	,	,	PUNCT
eurjchem-1701	69	14	24.76	24.76	NUM
eurjchem-1701	69	15	.	.	PUNCT
eurjchem-1701	69	16	found	find	VERB
eurjchem-1701	69	17	:	:	PUNCT
eurjchem-1701	70	1	c	c	X
eurjchem-1701	70	2	,	,	PUNCT
eurjchem-1701	70	3	37.10	37.10	NUM
eurjchem-1701	70	4	;	;	PUNCT
eurjchem-1701	70	5	h	h	NOUN
eurjchem-1701	70	6	,	,	PUNCT
eurjchem-1701	70	7	2.53	2.53	NUM
eurjchem-1701	70	8	;	;	PUNCT
eurjchem-1701	70	9	n	n	CCONJ
eurjchem-1701	70	10	,	,	PUNCT
eurjchem-1701	70	11	24.64	24.64	NUM
eurjchem-1701	70	12	%	%	NOUN
eurjchem-1701	70	13	.	.	PUNCT
eurjchem-1701	71	1	2.3.3	2.3.3	X
eurjchem-1701	71	2	.	.	X
eurjchem-1701	72	1	synthesis	synthesis	NOUN
eurjchem-1701	72	2	of	of	ADP
eurjchem-1701	72	3	1,2	1,2	NUM
eurjchem-1701	72	4	-	-	PUNCT
eurjchem-1701	72	5	dihydro-1	dihydro-1	NUM
eurjchem-1701	72	6	-	-	PUNCT
eurjchem-1701	72	7	phenyl-5-(thiophen-2	phenyl-5-(thiophen-2	NOUN
eurjchem-1701	72	8	-	-	PUNCT
eurjchem-1701	72	9	yl)-1	yl)-1	NOUN
eurjchem-1701	72	10	,	,	PUNCT
eurjchem-1701	72	11	2,4	2,4	NUM
eurjchem-1701	72	12	-	-	PUNCT
eurjchem-1701	72	13	triazole-3	triazole-3	NOUN
eurjchem-1701	72	14	-	-	PUNCT
eurjchem-1701	72	15	thione	thione	NOUN
eurjchem-1701	72	16	(	(	PUNCT
eurjchem-1701	72	17	4	4	NUM
eurjchem-1701	72	18	)	)	PUNCT
eurjchem-1701	72	19	a	a	DET
eurjchem-1701	72	20	mixture	mixture	NOUN
eurjchem-1701	72	21	of	of	ADP
eurjchem-1701	72	22	thiophene-2	thiophene-2	NOUN
eurjchem-1701	72	23	-	-	PUNCT
eurjchem-1701	72	24	carbonylisothiocyanate	carbonylisothiocyanate	NOUN
eurjchem-1701	72	25	(	(	PUNCT
eurjchem-1701	72	26	1	1	NUM
eurjchem-1701	72	27	)	)	PUNCT
eurjchem-1701	72	28	(	(	PUNCT
eurjchem-1701	72	29	3.40	3.40	NUM
eurjchem-1701	72	30	mol	mol	NOUN
eurjchem-1701	72	31	)	)	PUNCT
eurjchem-1701	72	32	and	and	CCONJ
eurjchem-1701	72	33	phenyl	phenyl	NOUN
eurjchem-1701	72	34	hydrazine	hydrazine	NOUN
eurjchem-1701	72	35	(	(	PUNCT
eurjchem-1701	72	36	3.40	3.40	NUM
eurjchem-1701	72	37	mol	mol	NOUN
eurjchem-1701	72	38	)	)	PUNCT
eurjchem-1701	72	39	in	in	ADP
eurjchem-1701	72	40	dioxane	dioxane	NOUN
eurjchem-1701	72	41	(	(	PUNCT
eurjchem-1701	72	42	50	50	NUM
eurjchem-1701	72	43	ml	ml	NOUN
eurjchem-1701	72	44	)	)	PUNCT
eurjchem-1701	72	45	was	be	AUX
eurjchem-1701	72	46	heated	heat	VERB
eurjchem-1701	72	47	under	under	ADP
eurjchem-1701	72	48	reflux	reflux	NOUN
eurjchem-1701	72	49	for	for	ADP
eurjchem-1701	72	50	2	2	NUM
eurjchem-1701	72	51	h.	h.	NOUN
eurjchem-1701	72	52	the	the	DET
eurjchem-1701	72	53	reaction	reaction	NOUN
eurjchem-1701	72	54	mixture	mixture	NOUN
eurjchem-1701	72	55	was	be	AUX
eurjchem-1701	72	56	poured	pour	VERB
eurjchem-1701	72	57	into	into	ADP
eurjchem-1701	72	58	water	water	NOUN
eurjchem-1701	72	59	.	.	PUNCT
eurjchem-1701	73	1	the	the	DET
eurjchem-1701	73	2	formed	form	VERB
eurjchem-1701	73	3	precipitate	precipitate	NOUN
eurjchem-1701	73	4	was	be	AUX
eurjchem-1701	73	5	filtered	filter	VERB
eurjchem-1701	73	6	off	off	ADP
eurjchem-1701	73	7	,	,	PUNCT
eurjchem-1701	73	8	washed	wash	VERB
eurjchem-1701	73	9	with	with	ADP
eurjchem-1701	73	10	water	water	NOUN
eurjchem-1701	73	11	,	,	PUNCT
eurjchem-1701	73	12	dried	dry	VERB
eurjchem-1701	73	13	and	and	CCONJ
eurjchem-1701	73	14	crystallized	crystallize	VERB
eurjchem-1701	73	15	from	from	ADP
eurjchem-1701	73	16	ethanol	ethanol	NOUN
eurjchem-1701	73	17	to	to	PART
eurjchem-1701	73	18	give	give	VERB
eurjchem-1701	73	19	compound	compound	NOUN
eurjchem-1701	73	20	4	4	NUM
eurjchem-1701	73	21	(	(	PUNCT
eurjchem-1701	73	22	scheme	scheme	NOUN
eurjchem-1701	73	23	1	1	NUM
eurjchem-1701	73	24	)	)	PUNCT
eurjchem-1701	73	25	.	.	PUNCT
eurjchem-1701	74	1	color	color	NOUN
eurjchem-1701	74	2	:	:	PUNCT
eurjchem-1701	74	3	yellow	yellow	ADJ
eurjchem-1701	74	4	.	.	PUNCT
eurjchem-1701	75	1	yield	yield	NOUN
eurjchem-1701	75	2	:	:	PUNCT
eurjchem-1701	75	3	63	63	NUM
eurjchem-1701	75	4	%	%	NOUN
eurjchem-1701	75	5	.	.	PUNCT
eurjchem-1701	76	1	m.p	m.p	PROPN
eurjchem-1701	76	2	.	.	PROPN
eurjchem-1701	76	3	:	:	PUNCT
eurjchem-1701	76	4	175176	175176	NUM
eurjchem-1701	76	5	°	°	SYM
eurjchem-1701	76	6	c	c	NOUN
eurjchem-1701	76	7	.	.	PUNCT
eurjchem-1701	76	8	ft	ft	PROPN
eurjchem-1701	76	9	-	-	PUNCT
eurjchem-1701	76	10	ir	ir	PROPN
eurjchem-1701	76	11	(	(	PUNCT
eurjchem-1701	76	12	kbr	kbr	PROPN
eurjchem-1701	76	13	,	,	PUNCT
eurjchem-1701	76	14	ν	ν	PROPN
eurjchem-1701	76	15	,	,	PUNCT
eurjchem-1701	76	16	cm-1	cm-1	NUM
eurjchem-1701	76	17	):	):	PUNCT
eurjchem-1701	76	18	3313	3313	NUM
eurjchem-1701	76	19	(	(	PUNCT
eurjchem-1701	76	20	nh	nh	NOUN
eurjchem-1701	76	21	)	)	PUNCT
eurjchem-1701	76	22	,	,	PUNCT
eurjchem-1701	76	23	1635	1635	NUM
eurjchem-1701	76	24	(	(	PUNCT
eurjchem-1701	76	25	c	c	NOUN
eurjchem-1701	76	26	=	=	SYM
eurjchem-1701	76	27	n	n	NUM
eurjchem-1701	76	28	)	)	PUNCT
eurjchem-1701	76	29	,	,	PUNCT
eurjchem-1701	76	30	1615	1615	NUM
eurjchem-1701	76	31	(	(	PUNCT
eurjchem-1701	76	32	c	c	NOUN
eurjchem-1701	76	33	=	=	SYM
eurjchem-1701	76	34	c	c	NOUN
eurjchem-1701	76	35	)	)	PUNCT
eurjchem-1701	76	36	.	.	PUNCT
eurjchem-1701	77	1	1h	1h	NUM
eurjchem-1701	77	2	nmr	nmr	NOUN
eurjchem-1701	77	3	(	(	PUNCT
eurjchem-1701	77	4	300	300	NUM
eurjchem-1701	77	5	mhz	mhz	NOUN
eurjchem-1701	77	6	,	,	PUNCT
eurjchem-1701	77	7	dmso	dmso	NOUN
eurjchem-1701	77	8	-	-	NOUN
eurjchem-1701	77	9	d6	d6	NOUN
eurjchem-1701	77	10	,	,	PUNCT
eurjchem-1701	77	11	δ	δ	PROPN
eurjchem-1701	77	12	,	,	PUNCT
eurjchem-1701	77	13	ppm	ppm	NOUN
eurjchem-1701	77	14	):	):	PUNCT
eurjchem-1701	77	15	7.93	7.93	NUM
eurjchem-1701	77	16	-	-	SYM
eurjchem-1701	77	17	6.72	6.72	NUM
eurjchem-1701	77	18	(	(	PUNCT
eurjchem-1701	77	19	m	m	PROPN
eurjchem-1701	77	20	,	,	PUNCT
eurjchem-1701	77	21	8h	8h	NUM
eurjchem-1701	77	22	,	,	PUNCT
eurjchem-1701	77	23	arh	arh	PROPN
eurjchem-1701	77	24	’s	’s	PART
eurjchem-1701	77	25	+	+	NUM
eurjchem-1701	77	26	thiophene	thiophene	NOUN
eurjchem-1701	77	27	protons	proton	NOUN
eurjchem-1701	77	28	)	)	PUNCT
eurjchem-1701	77	29	,	,	PUNCT
eurjchem-1701	77	30	10.37	10.37	NUM
eurjchem-1701	77	31	(	(	PUNCT
eurjchem-1701	77	32	s	s	PROPN
eurjchem-1701	77	33	,	,	PUNCT
eurjchem-1701	77	34	1h	1h	NUM
eurjchem-1701	77	35	,	,	PUNCT
eurjchem-1701	77	36	d2o	d2o	NOUN
eurjchem-1701	77	37	exchangeable	exchangeable	ADJ
eurjchem-1701	77	38	,	,	PUNCT
eurjchem-1701	77	39	nh	nh	PROPN
eurjchem-1701	77	40	)	)	PUNCT
eurjchem-1701	77	41	.	.	PUNCT
eurjchem-1701	78	1	1h	1h	NUM
eurjchem-1701	78	2	nmr	nmr	NOUN
eurjchem-1701	78	3	(	(	PUNCT
eurjchem-1701	78	4	300	300	NUM
eurjchem-1701	78	5	mhz	mhz	NOUN
eurjchem-1701	78	6	,	,	PUNCT
eurjchem-1701	78	7	dmso	dmso	NOUN
eurjchem-1701	78	8	-	-	NOUN
eurjchem-1701	78	9	d6	d6	NOUN
eurjchem-1701	78	10	,	,	PUNCT
eurjchem-1701	78	11	δ	δ	PROPN
eurjchem-1701	78	12	,	,	PUNCT
eurjchem-1701	78	13	h	h	NOUN
eurjchem-1701	78	14	/	/	SYM
eurjchem-1701	78	15	d	d	NOUN
eurjchem-1701	78	16	-	-	NOUN
eurjchem-1701	78	17	exchange	exchange	NOUN
eurjchem-1701	78	18	,	,	PUNCT
eurjchem-1701	78	19	ppm	ppm	NOUN
eurjchem-1701	78	20	):	):	PUNCT
eurjchem-1701	78	21	7.93	7.93	NUM
eurjchem-1701	78	22	-	-	SYM
eurjchem-1701	78	23	6.72	6.72	NUM
eurjchem-1701	78	24	(	(	PUNCT
eurjchem-1701	78	25	m	m	PROPN
eurjchem-1701	78	26	,	,	PUNCT
eurjchem-1701	78	27	8h	8h	NUM
eurjchem-1701	78	28	,	,	PUNCT
eurjchem-1701	78	29	arh	arh	PROPN
eurjchem-1701	78	30	’s	’s	PART
eurjchem-1701	78	31	+	+	NUM
eurjchem-1701	78	32	thiophene	thiophene	NOUN
eurjchem-1701	78	33	protons	proton	NOUN
eurjchem-1701	78	34	)	)	PUNCT
eurjchem-1701	78	35	.	.	PUNCT
eurjchem-1701	79	1	13c	13c	NOUN
eurjchem-1701	79	2	nmr	nmr	NOUN
eurjchem-1701	79	3	(	(	PUNCT
eurjchem-1701	79	4	75.4	75.4	NUM
eurjchem-1701	79	5	mhz	mhz	NOUN
eurjchem-1701	79	6	,	,	PUNCT
eurjchem-1701	79	7	dmso	dmso	NOUN
eurjchem-1701	79	8	-	-	NOUN
eurjchem-1701	79	9	d6	d6	NOUN
eurjchem-1701	79	10	,	,	PUNCT
eurjchem-1701	79	11	δ	δ	PROPN
eurjchem-1701	79	12	,	,	PUNCT
eurjchem-1701	79	13	ppm	ppm	NUM
eurjchem-1701	79	14	):	):	PUNCT
eurjchem-1701	79	15	166.6	166.6	NUM
eurjchem-1701	79	16	(	(	PUNCT
eurjchem-1701	79	17	1c	1c	NOUN
eurjchem-1701	79	18	,	,	PUNCT
eurjchem-1701	79	19	ncs	ncs	NOUN
eurjchem-1701	79	20	)	)	PUNCT
eurjchem-1701	79	21	,	,	PUNCT
eurjchem-1701	79	22	156.4	156.4	NUM
eurjchem-1701	79	23	(	(	PUNCT
eurjchem-1701	79	24	1c	1c	X
eurjchem-1701	79	25	,	,	PUNCT
eurjchem-1701	79	26	ncn	ncn	NOUN
eurjchem-1701	79	27	)	)	PUNCT
eurjchem-1701	79	28	,	,	PUNCT
eurjchem-1701	79	29	136.5	136.5	NUM
eurjchem-1701	79	30	,	,	PUNCT
eurjchem-1701	79	31	129.4	129.4	NUM
eurjchem-1701	79	32	,	,	PUNCT
eurjchem-1701	79	33	129.0	129.0	NUM
eurjchem-1701	79	34	,	,	PUNCT
eurjchem-1701	79	35	128.6	128.6	NUM
eurjchem-1701	79	36	,	,	PUNCT
eurjchem-1701	79	37	128.1	128.1	NUM
eurjchem-1701	79	38	,	,	PUNCT
eurjchem-1701	79	39	127.7	127.7	NUM
eurjchem-1701	79	40	,	,	PUNCT
eurjchem-1701	79	41	121.1	121.1	NUM
eurjchem-1701	79	42	,	,	PUNCT
eurjchem-1701	79	43	119.2	119.2	NUM
eurjchem-1701	79	44	(	(	PUNCT
eurjchem-1701	79	45	ar	ar	NOUN
eurjchem-1701	79	46	-	-	NOUN
eurjchem-1701	79	47	c	c	NOUN
eurjchem-1701	79	48	)	)	PUNCT
eurjchem-1701	79	49	.	.	PUNCT
eurjchem-1701	80	1	ms	ms	NOUN
eurjchem-1701	80	2	(	(	PUNCT
eurjchem-1701	80	3	ei	ei	PROPN
eurjchem-1701	80	4	,	,	PUNCT
eurjchem-1701	80	5	m	m	PROPN
eurjchem-1701	80	6	/	/	SYM
eurjchem-1701	80	7	z	z	PROPN
eurjchem-1701	80	8	(	(	PUNCT
eurjchem-1701	80	9	%	%	NOUN
eurjchem-1701	80	10	)	)	PUNCT
eurjchem-1701	80	11	):	):	PUNCT
eurjchem-1701	80	12	258	258	NUM
eurjchem-1701	80	13	(	(	PUNCT
eurjchem-1701	80	14	m+	m+	NUM
eurjchem-1701	80	15	,	,	PUNCT
eurjchem-1701	80	16	20	20	NUM
eurjchem-1701	80	17	)	)	PUNCT
eurjchem-1701	80	18	,	,	PUNCT
eurjchem-1701	80	19	217	217	NUM
eurjchem-1701	80	20	(	(	PUNCT
eurjchem-1701	80	21	30	30	NUM
eurjchem-1701	80	22	)	)	PUNCT
eurjchem-1701	80	23	,	,	PUNCT
eurjchem-1701	80	24	110	110	NUM
eurjchem-1701	80	25	(	(	PUNCT
eurjchem-1701	80	26	100	100	NUM
eurjchem-1701	80	27	)	)	PUNCT
eurjchem-1701	80	28	,	,	PUNCT
eurjchem-1701	80	29	77	77	NUM
eurjchem-1701	80	30	(	(	PUNCT
eurjchem-1701	80	31	20	20	NUM
eurjchem-1701	80	32	)	)	PUNCT
eurjchem-1701	80	33	.	.	PUNCT
eurjchem-1701	81	1	anal	anal	PROPN
eurjchem-1701	81	2	.	.	PUNCT
eurjchem-1701	81	3	calcd	calcd	NOUN
eurjchem-1701	81	4	.	.	PUNCT
eurjchem-1701	82	1	for	for	SCONJ
eurjchem-1701	82	2	c12h9n3s2	c12h9n3s2	NOUN
eurjchem-1701	82	3	:	:	PUNCT
eurjchem-1701	82	4	c	c	X
eurjchem-1701	82	5	,	,	PUNCT
eurjchem-1701	82	6	55.57	55.57	NUM
eurjchem-1701	82	7	;	;	PUNCT
eurjchem-1701	82	8	h	h	NOUN
eurjchem-1701	82	9	,	,	PUNCT
eurjchem-1701	82	10	3.50	3.50	NUM
eurjchem-1701	82	11	;	;	PUNCT
eurjchem-1701	82	12	n	n	CCONJ
eurjchem-1701	82	13	,	,	PUNCT
eurjchem-1701	82	14	16.20	16.20	NUM
eurjchem-1701	82	15	.	.	PUNCT
eurjchem-1701	82	16	found	find	VERB
eurjchem-1701	82	17	:	:	PUNCT
eurjchem-1701	83	1	c	c	X
eurjchem-1701	83	2	,	,	PUNCT
eurjchem-1701	83	3	55.49	55.49	NUM
eurjchem-1701	83	4	;	;	PUNCT
eurjchem-1701	83	5	h	h	NOUN
eurjchem-1701	83	6	,	,	PUNCT
eurjchem-1701	83	7	3.45	3.45	NUM
eurjchem-1701	83	8	;	;	PUNCT
eurjchem-1701	83	9	n	n	CCONJ
eurjchem-1701	83	10	,	,	PUNCT
eurjchem-1701	83	11	15.90	15.90	NUM
eurjchem-1701	83	12	%	%	NOUN
eurjchem-1701	83	13	.	.	PUNCT
eurjchem-1701	84	1	2.3.4	2.3.4	X
eurjchem-1701	84	2	.	.	PUNCT
eurjchem-1701	84	3	synthesis	synthesis	NOUN
eurjchem-1701	84	4	of	of	ADP
eurjchem-1701	84	5	n-(1	n-(1	PROPN
eurjchem-1701	84	6	-	-	PUNCT
eurjchem-1701	84	7	phenylhydrazinecarbonothioyl)thio	phenylhydrazinecarbonothioyl)thio	ADJ
eurjchem-1701	84	8	phene-2	phene-2	ADJ
eurjchem-1701	84	9	-	-	PUNCT
eurjchem-1701	84	10	carboxamide	carboxamide	NOUN
eurjchem-1701	84	11	hydrochloride	hydrochloride	NOUN
eurjchem-1701	84	12	(	(	PUNCT
eurjchem-1701	84	13	5	5	NUM
eurjchem-1701	84	14	)	)	PUNCT
eurjchem-1701	84	15	a	a	DET
eurjchem-1701	84	16	mixture	mixture	NOUN
eurjchem-1701	84	17	of	of	ADP
eurjchem-1701	84	18	thiophene-2	thiophene-2	NOUN
eurjchem-1701	84	19	-	-	PUNCT
eurjchem-1701	84	20	carbonylisothiocyanate	carbonylisothiocyanate	NOUN
eurjchem-1701	84	21	(	(	PUNCT
eurjchem-1701	84	22	1	1	NUM
eurjchem-1701	84	23	)	)	PUNCT
eurjchem-1701	84	24	(	(	PUNCT
eurjchem-1701	84	25	10.0	10.0	NUM
eurjchem-1701	84	26	mol	mol	NOUN
eurjchem-1701	84	27	)	)	PUNCT
eurjchem-1701	84	28	and	and	CCONJ
eurjchem-1701	84	29	phenyl	phenyl	NOUN
eurjchem-1701	84	30	hydrazine	hydrazine	NOUN
eurjchem-1701	84	31	hydrochloride	hydrochloride	NOUN
eurjchem-1701	84	32	(	(	PUNCT
eurjchem-1701	84	33	10.0	10.0	NUM
eurjchem-1701	84	34	mol	mol	NOUN
eurjchem-1701	84	35	)	)	PUNCT
eurjchem-1701	84	36	in	in	ADP
eurjchem-1701	84	37	dioxane	dioxane	NOUN
eurjchem-1701	84	38	:	:	PUNCT
eurjchem-1701	84	39	water	water	NOUN
eurjchem-1701	84	40	(	(	PUNCT
eurjchem-1701	84	41	1:1	1:1	NUM
eurjchem-1701	84	42	,	,	PUNCT
eurjchem-1701	84	43	v	v	NOUN
eurjchem-1701	84	44	:	:	SYM
eurjchem-1701	84	45	v	v	NOUN
eurjchem-1701	84	46	)	)	PUNCT
eurjchem-1701	84	47	(	(	PUNCT
eurjchem-1701	84	48	50	50	NUM
eurjchem-1701	84	49	ml	ml	NOUN
eurjchem-1701	84	50	)	)	PUNCT
eurjchem-1701	84	51	was	be	AUX
eurjchem-1701	84	52	stirred	stir	VERB
eurjchem-1701	84	53	at	at	ADP
eurjchem-1701	84	54	room	room	NOUN
eurjchem-1701	84	55	temperature	temperature	NOUN
eurjchem-1701	84	56	for	for	ADP
eurjchem-1701	84	57	1	1	NUM
eurjchem-1701	84	58	h.	h.	NOUN
eurjchem-1701	84	59	the	the	DET
eurjchem-1701	84	60	reaction	reaction	NOUN
eurjchem-1701	84	61	mixture	mixture	NOUN
eurjchem-1701	84	62	was	be	AUX
eurjchem-1701	84	63	poured	pour	VERB
eurjchem-1701	84	64	into	into	ADP
eurjchem-1701	84	65	cold	cold	ADJ
eurjchem-1701	84	66	water	water	NOUN
eurjchem-1701	84	67	.	.	PUNCT
eurjchem-1701	85	1	the	the	DET
eurjchem-1701	85	2	formed	form	VERB
eurjchem-1701	85	3	precipitatet	precipitatet	NOUN
eurjchem-1701	85	4	was	be	AUX
eurjchem-1701	85	5	filtered	filter	VERB
eurjchem-1701	85	6	off	off	ADP
eurjchem-1701	85	7	,	,	PUNCT
eurjchem-1701	85	8	washed	wash	VERB
eurjchem-1701	85	9	with	with	ADP
eurjchem-1701	85	10	cold	cold	ADJ
eurjchem-1701	85	11	water	water	NOUN
eurjchem-1701	85	12	,	,	PUNCT
eurjchem-1701	85	13	dried	dry	VERB
eurjchem-1701	85	14	and	and	CCONJ
eurjchem-1701	85	15	crystallized	crystallize	VERB
eurjchem-1701	85	16	from	from	ADP
eurjchem-1701	85	17	ethanol	ethanol	NOUN
eurjchem-1701	85	18	to	to	PART
eurjchem-1701	85	19	give	give	VERB
eurjchem-1701	85	20	compound	compound	NOUN
eurjchem-1701	85	21	5	5	NUM
eurjchem-1701	85	22	(	(	PUNCT
eurjchem-1701	85	23	scheme	scheme	NOUN
eurjchem-1701	85	24	2	2	NUM
eurjchem-1701	85	25	)	)	PUNCT
eurjchem-1701	85	26	.	.	PUNCT
eurjchem-1701	86	1	color	color	NOUN
eurjchem-1701	86	2	:	:	PUNCT
eurjchem-1701	86	3	white	white	ADJ
eurjchem-1701	86	4	.	.	PUNCT
eurjchem-1701	87	1	yield	yield	NOUN
eurjchem-1701	87	2	:	:	PUNCT
eurjchem-1701	87	3	54	54	NUM
eurjchem-1701	87	4	%	%	NOUN
eurjchem-1701	87	5	.	.	PUNCT
eurjchem-1701	88	1	m.p	m.p	PROPN
eurjchem-1701	88	2	.	.	PROPN
eurjchem-1701	88	3	:	:	PUNCT
eurjchem-1701	89	1	268269	268269	NUM
eurjchem-1701	89	2	°	°	SYM
eurjchem-1701	89	3	c	c	NOUN
eurjchem-1701	89	4	.	.	PUNCT
eurjchem-1701	89	5	ft	ft	PROPN
eurjchem-1701	89	6	-	-	PUNCT
eurjchem-1701	89	7	ir	ir	PROPN
eurjchem-1701	89	8	(	(	PUNCT
eurjchem-1701	89	9	kbr	kbr	PROPN
eurjchem-1701	89	10	,	,	PUNCT
eurjchem-1701	89	11	ν	ν	PROPN
eurjchem-1701	89	12	,	,	PUNCT
eurjchem-1701	89	13	cm-1	cm-1	NUM
eurjchem-1701	89	14	):	):	PUNCT
eurjchem-1701	89	15	3406	3406	NUM
eurjchem-1701	89	16	,	,	PUNCT
eurjchem-1701	89	17	3280	3280	NUM
eurjchem-1701	89	18	,	,	PUNCT
eurjchem-1701	89	19	(	(	PUNCT
eurjchem-1701	89	20	nh2	nh2	PROPN
eurjchem-1701	89	21	,	,	PUNCT
eurjchem-1701	89	22	nh	nh	PROPN
eurjchem-1701	89	23	)	)	PUNCT
eurjchem-1701	89	24	,	,	PUNCT
eurjchem-1701	89	25	1665	1665	NUM
eurjchem-1701	89	26	(	(	PUNCT
eurjchem-1701	89	27	c	c	NOUN
eurjchem-1701	89	28	=	=	NOUN
eurjchem-1701	89	29	o	o	NOUN
eurjchem-1701	89	30	)	)	PUNCT
eurjchem-1701	89	31	,	,	PUNCT
eurjchem-1701	89	32	1635	1635	NUM
eurjchem-1701	89	33	(	(	PUNCT
eurjchem-1701	89	34	c	c	NOUN
eurjchem-1701	89	35	=	=	SYM
eurjchem-1701	89	36	c	c	NOUN
eurjchem-1701	89	37	)	)	PUNCT
eurjchem-1701	89	38	.	.	PUNCT
eurjchem-1701	90	1	1h	1h	NUM
eurjchem-1701	90	2	nmr	nmr	NOUN
eurjchem-1701	90	3	(	(	PUNCT
eurjchem-1701	90	4	300	300	NUM
eurjchem-1701	90	5	mhz	mhz	NOUN
eurjchem-1701	90	6	,	,	PUNCT
eurjchem-1701	90	7	dmso	dmso	NOUN
eurjchem-1701	90	8	-	-	NOUN
eurjchem-1701	90	9	d6	d6	NOUN
eurjchem-1701	90	10	,	,	PUNCT
eurjchem-1701	90	11	δ	δ	PROPN
eurjchem-1701	90	12	,	,	PUNCT
eurjchem-1701	90	13	ppm	ppm	NOUN
eurjchem-1701	90	14	):	):	PUNCT
eurjchem-1701	90	15	7.987.24	7.987.24	NUM
eurjchem-1701	90	16	(	(	PUNCT
eurjchem-1701	90	17	m	m	PROPN
eurjchem-1701	90	18	,	,	PUNCT
eurjchem-1701	90	19	8h	8h	NUM
eurjchem-1701	90	20	,	,	PUNCT
eurjchem-1701	90	21	arh	arh	PROPN
eurjchem-1701	90	22	’s	’s	PART
eurjchem-1701	90	23	+	+	NUM
eurjchem-1701	90	24	thiophene	thiophene	NOUN
eurjchem-1701	90	25	protons	proton	NOUN
eurjchem-1701	90	26	)	)	PUNCT
eurjchem-1701	90	27	,	,	PUNCT
eurjchem-1701	90	28	11.62	11.62	NUM
eurjchem-1701	90	29	(	(	PUNCT
eurjchem-1701	90	30	s	s	PROPN
eurjchem-1701	90	31	,	,	PUNCT
eurjchem-1701	90	32	2h	2h	NUM
eurjchem-1701	90	33	,	,	PUNCT
eurjchem-1701	90	34	nh2	nh2	PROPN
eurjchem-1701	90	35	)	)	PUNCT
eurjchem-1701	90	36	,	,	PUNCT
eurjchem-1701	90	37	14.41	14.41	NUM
eurjchem-1701	90	38	(	(	PUNCT
eurjchem-1701	90	39	s	s	PROPN
eurjchem-1701	90	40	,	,	PUNCT
eurjchem-1701	90	41	1h	1h	NUM
eurjchem-1701	90	42	,	,	PUNCT
eurjchem-1701	90	43	nh	nh	PROPN
eurjchem-1701	90	44	)	)	PUNCT
eurjchem-1701	90	45	.	.	PUNCT
eurjchem-1701	91	1	2.3.5	2.3.5	NUM
eurjchem-1701	91	2	.	.	PUNCT
eurjchem-1701	91	3	synthesis	synthesis	NOUN
eurjchem-1701	91	4	of	of	ADP
eurjchem-1701	91	5	n-(6	n-(6	NOUN
eurjchem-1701	91	6	-	-	PUNCT
eurjchem-1701	91	7	oxo-2	oxo-2	NOUN
eurjchem-1701	91	8	-	-	PUNCT
eurjchem-1701	91	9	phenyl-5,6	phenyl-5,6	NOUN
eurjchem-1701	91	10	-	-	PUNCT
eurjchem-1701	91	11	dihydro-1hfuro[2,3	dihydro-1hfuro[2,3	NOUN
eurjchem-1701	91	12	-	-	NOUN
eurjchem-1701	91	13	e][1,3,4]thiadiazin-3(2h)-ylidene)thiophene-2carboxamide	e][1,3,4]thiadiazin-3(2h)-ylidene)thiophene-2carboxamide	NOUN
eurjchem-1701	91	14	(	(	PUNCT
eurjchem-1701	91	15	6	6	NUM
eurjchem-1701	91	16	)	)	PUNCT
eurjchem-1701	91	17	a	a	DET
eurjchem-1701	91	18	mixture	mixture	NOUN
eurjchem-1701	91	19	of	of	ADP
eurjchem-1701	91	20	n-(1	n-(1	NOUN
eurjchem-1701	91	21	-	-	PUNCT
eurjchem-1701	91	22	phenylhydrazinecarbonothioyl)thiophene-2	phenylhydrazinecarbonothioyl)thiophene-2	PRON
eurjchem-1701	91	23	-	-	PUNCT
eurjchem-1701	91	24	carboxamide	carboxamide	NOUN
eurjchem-1701	91	25	hydrochloride	hydrochloride	NOUN
eurjchem-1701	91	26	(	(	PUNCT
eurjchem-1701	91	27	5	5	NUM
eurjchem-1701	91	28	)	)	PUNCT
eurjchem-1701	91	29	(	(	PUNCT
eurjchem-1701	91	30	1.50	1.50	NUM
eurjchem-1701	91	31	mol	mol	NOUN
eurjchem-1701	91	32	)	)	PUNCT
eurjchem-1701	91	33	,	,	PUNCT
eurjchem-1701	91	34	maleic	maleic	VERB
eurjchem-1701	91	35	anhydride	anhydride	NOUN
eurjchem-1701	91	36	(	(	PUNCT
eurjchem-1701	91	37	1.50	1.50	NUM
eurjchem-1701	91	38	mol	mol	NOUN
eurjchem-1701	91	39	)	)	PUNCT
eurjchem-1701	91	40	and	and	CCONJ
eurjchem-1701	91	41	triethyl	triethyl	PROPN
eurjchem-1701	91	42	amine	amine	PROPN
eurjchem-1701	91	43	(	(	PUNCT
eurjchem-1701	91	44	1.50	1.50	NUM
eurjchem-1701	91	45	mole	mole	NOUN
eurjchem-1701	91	46	)	)	PUNCT
eurjchem-1701	91	47	in	in	ADP
eurjchem-1701	91	48	dimethyl	dimethyl	PROPN
eurjchem-1701	91	49	formamide	formamide	ADV
eurjchem-1701	91	50	(	(	PUNCT
eurjchem-1701	91	51	20	20	NUM
eurjchem-1701	91	52	ml	ml	NOUN
eurjchem-1701	91	53	)	)	PUNCT
eurjchem-1701	91	54	was	be	AUX
eurjchem-1701	91	55	heated	heat	VERB
eurjchem-1701	91	56	under	under	ADP
eurjchem-1701	91	57	reflux	reflux	NOUN
eurjchem-1701	91	58	for	for	ADP
eurjchem-1701	91	59	6	6	NUM
eurjchem-1701	91	60	h.	h.	NOUN
eurjchem-1701	91	61	the	the	DET
eurjchem-1701	91	62	reaction	reaction	NOUN
eurjchem-1701	91	63	mixture	mixture	NOUN
eurjchem-1701	91	64	was	be	AUX
eurjchem-1701	91	65	neutralized	neutralize	VERB
eurjchem-1701	91	66	by	by	ADP
eurjchem-1701	91	67	10	10	NUM
eurjchem-1701	91	68	%	%	NOUN
eurjchem-1701	91	69	hcl	hcl	PROPN
eurjchem-1701	91	70	.	.	PUNCT
eurjchem-1701	92	1	the	the	DET
eurjchem-1701	92	2	formed	form	VERB
eurjchem-1701	92	3	precipitate	precipitate	NOUN
eurjchem-1701	92	4	was	be	AUX
eurjchem-1701	92	5	filtered	filter	VERB
eurjchem-1701	92	6	off	off	ADP
eurjchem-1701	92	7	,	,	PUNCT
eurjchem-1701	92	8	dried	dry	VERB
eurjchem-1701	92	9	and	and	CCONJ
eurjchem-1701	92	10	crystallized	crystallize	VERB
eurjchem-1701	92	11	from	from	ADP
eurjchem-1701	92	12	ethanol	ethanol	NOUN
eurjchem-1701	92	13	to	to	PART
eurjchem-1701	92	14	give	give	VERB
eurjchem-1701	92	15	compound	compound	NOUN
eurjchem-1701	92	16	6	6	NUM
eurjchem-1701	92	17	(	(	PUNCT
eurjchem-1701	92	18	scheme	scheme	NOUN
eurjchem-1701	92	19	2	2	NUM
eurjchem-1701	92	20	and	and	CCONJ
eurjchem-1701	92	21	3	3	NUM
eurjchem-1701	92	22	)	)	PUNCT
eurjchem-1701	92	23	.	.	PUNCT
eurjchem-1701	93	1	color	color	NOUN
eurjchem-1701	93	2	:	:	PUNCT
eurjchem-1701	93	3	brown	brown	ADJ
eurjchem-1701	93	4	.	.	PUNCT
eurjchem-1701	94	1	yield	yield	NOUN
eurjchem-1701	94	2	:	:	PUNCT
eurjchem-1701	94	3	61	61	NUM
eurjchem-1701	94	4	%	%	NOUN
eurjchem-1701	94	5	.	.	PUNCT
eurjchem-1701	95	1	m.p	m.p	PROPN
eurjchem-1701	95	2	.	.	PROPN
eurjchem-1701	95	3	:	:	PUNCT
eurjchem-1701	96	1	288	288	NUM
eurjchem-1701	96	2	-	-	SYM
eurjchem-1701	96	3	289	289	NUM
eurjchem-1701	96	4	°	°	NUM
eurjchem-1701	96	5	c	c	NOUN
eurjchem-1701	96	6	.	.	PUNCT
eurjchem-1701	96	7	ft	ft	PROPN
eurjchem-1701	96	8	-	-	PUNCT
eurjchem-1701	96	9	ir	ir	PROPN
eurjchem-1701	96	10	(	(	PUNCT
eurjchem-1701	96	11	kbr	kbr	PROPN
eurjchem-1701	96	12	,	,	PUNCT
eurjchem-1701	96	13	ν	ν	PROPN
eurjchem-1701	96	14	,	,	PUNCT
eurjchem-1701	96	15	cm-1	cm-1	NUM
eurjchem-1701	96	16	):	):	PUNCT
eurjchem-1701	96	17	3631	3631	NUM
eurjchem-1701	96	18	,	,	PUNCT
eurjchem-1701	96	19	3217	3217	NUM
eurjchem-1701	96	20	(	(	PUNCT
eurjchem-1701	96	21	nh	nh	NOUN
eurjchem-1701	96	22	)	)	PUNCT
eurjchem-1701	96	23	,	,	PUNCT
eurjchem-1701	96	24	1723	1723	NUM
eurjchem-1701	96	25	(	(	PUNCT
eurjchem-1701	96	26	c	c	NOUN
eurjchem-1701	96	27	=	=	NOUN
eurjchem-1701	96	28	o	o	NOUN
eurjchem-1701	96	29	)	)	PUNCT
eurjchem-1701	96	30	(	(	PUNCT
eurjchem-1701	96	31	ester	ester	NOUN
eurjchem-1701	96	32	)	)	PUNCT
eurjchem-1701	96	33	,	,	PUNCT
eurjchem-1701	96	34	1667	1667	NUM
eurjchem-1701	96	35	(	(	PUNCT
eurjchem-1701	96	36	c	c	NOUN
eurjchem-1701	96	37	=	=	NOUN
eurjchem-1701	96	38	o	o	NOUN
eurjchem-1701	96	39	)	)	PUNCT
eurjchem-1701	96	40	(	(	PUNCT
eurjchem-1701	96	41	amide	amide	NOUN
eurjchem-1701	96	42	)	)	PUNCT
eurjchem-1701	96	43	,	,	PUNCT
eurjchem-1701	96	44	1631	1631	NUM
eurjchem-1701	96	45	(	(	PUNCT
eurjchem-1701	96	46	c	c	NOUN
eurjchem-1701	96	47	=	=	SYM
eurjchem-1701	96	48	n	n	NUM
eurjchem-1701	96	49	)	)	PUNCT
eurjchem-1701	96	50	,	,	PUNCT
eurjchem-1701	96	51	1617	1617	NUM
eurjchem-1701	96	52	(	(	PUNCT
eurjchem-1701	96	53	c	c	NOUN
eurjchem-1701	96	54	=	=	SYM
eurjchem-1701	96	55	c	c	NOUN
eurjchem-1701	96	56	)	)	PUNCT
eurjchem-1701	96	57	,	,	PUNCT
eurjchem-1701	96	58	1244	1244	NUM
eurjchem-1701	96	59	(	(	PUNCT
eurjchem-1701	96	60	c	c	NOUN
eurjchem-1701	96	61	-	-	PUNCT
eurjchem-1701	96	62	o	o	NOUN
eurjchem-1701	96	63	)	)	PUNCT
eurjchem-1701	96	64	.	.	PUNCT
eurjchem-1701	97	1	1h	1h	NUM
eurjchem-1701	97	2	nmr	nmr	NOUN
eurjchem-1701	97	3	(	(	PUNCT
eurjchem-1701	97	4	300	300	NUM
eurjchem-1701	97	5	mhz	mhz	NOUN
eurjchem-1701	97	6	,	,	PUNCT
eurjchem-1701	97	7	dmso	dmso	NOUN
eurjchem-1701	97	8	-	-	NOUN
eurjchem-1701	97	9	d6	d6	NOUN
eurjchem-1701	97	10	,	,	PUNCT
eurjchem-1701	97	11	δ	δ	PROPN
eurjchem-1701	97	12	,	,	PUNCT
eurjchem-1701	97	13	ppm	ppm	NUM
eurjchem-1701	97	14	):	):	PUNCT
eurjchem-1701	97	15	2.95	2.95	NUM
eurjchem-1701	97	16	(	(	PUNCT
eurjchem-1701	97	17	s	s	PROPN
eurjchem-1701	97	18	,	,	PUNCT
eurjchem-1701	97	19	2h	2h	NUM
eurjchem-1701	97	20	,	,	PUNCT
eurjchem-1701	97	21	ch2co	ch2co	NOUN
eurjchem-1701	97	22	)	)	PUNCT
eurjchem-1701	97	23	,	,	PUNCT
eurjchem-1701	97	24	7.98	7.98	NUM
eurjchem-1701	97	25	-	-	SYM
eurjchem-1701	97	26	7.15	7.15	NUM
eurjchem-1701	97	27	(	(	PUNCT
eurjchem-1701	97	28	m	m	PROPN
eurjchem-1701	97	29	,	,	PUNCT
eurjchem-1701	97	30	8h	8h	NUM
eurjchem-1701	97	31	,	,	PUNCT
eurjchem-1701	97	32	arh	arh	PROPN
eurjchem-1701	97	33	’s	’s	PART
eurjchem-1701	97	34	+	+	NUM
eurjchem-1701	97	35	thiophene	thiophene	NOUN
eurjchem-1701	97	36	protons	proton	NOUN
eurjchem-1701	97	37	)	)	PUNCT
eurjchem-1701	97	38	,	,	PUNCT
eurjchem-1701	97	39	12.65	12.65	NUM
eurjchem-1701	97	40	(	(	PUNCT
eurjchem-1701	97	41	s	s	PROPN
eurjchem-1701	97	42	,	,	PUNCT
eurjchem-1701	97	43	1h	1h	NUM
eurjchem-1701	97	44	,	,	PUNCT
eurjchem-1701	97	45	d2o	d2o	NOUN
eurjchem-1701	97	46	exchangeable	exchangeable	ADJ
eurjchem-1701	97	47	,	,	PUNCT
eurjchem-1701	97	48	nh	nh	PROPN
eurjchem-1701	97	49	)	)	PUNCT
eurjchem-1701	97	50	.	.	PUNCT
eurjchem-1701	98	1	13c	13c	NOUN
eurjchem-1701	98	2	nmr	nmr	NOUN
eurjchem-1701	98	3	(	(	PUNCT
eurjchem-1701	98	4	75.4	75.4	NUM
eurjchem-1701	98	5	mhz	mhz	NOUN
eurjchem-1701	98	6	,	,	PUNCT
eurjchem-1701	98	7	dmso	dmso	NOUN
eurjchem-1701	98	8	-	-	NOUN
eurjchem-1701	98	9	d6	d6	NOUN
eurjchem-1701	98	10	,	,	PUNCT
eurjchem-1701	98	11	δ	δ	PROPN
eurjchem-1701	98	12	,	,	PUNCT
eurjchem-1701	98	13	ppm	ppm	NOUN
eurjchem-1701	98	14	):	):	PUNCT
eurjchem-1701	98	15	168.3	168.3	NUM
eurjchem-1701	98	16	,	,	PUNCT
eurjchem-1701	98	17	165.2	165.2	NUM
eurjchem-1701	98	18	(	(	PUNCT
eurjchem-1701	98	19	2c	2c	NOUN
eurjchem-1701	98	20	,	,	PUNCT
eurjchem-1701	98	21	2c	2c	NOUN
eurjchem-1701	98	22	=	=	SYM
eurjchem-1701	98	23	o	o	NOUN
eurjchem-1701	98	24	)	)	PUNCT
eurjchem-1701	98	25	,	,	PUNCT
eurjchem-1701	98	26	156.7	156.7	NUM
eurjchem-1701	98	27	(	(	PUNCT
eurjchem-1701	98	28	1c	1c	X
eurjchem-1701	98	29	,	,	PUNCT
eurjchem-1701	98	30	ncn	ncn	NOUN
eurjchem-1701	98	31	)	)	PUNCT
eurjchem-1701	98	32	,	,	PUNCT
eurjchem-1701	98	33	143.1	143.1	NUM
eurjchem-1701	98	34	,	,	PUNCT
eurjchem-1701	98	35	146.0	146.0	NUM
eurjchem-1701	98	36	,	,	PUNCT
eurjchem-1701	98	37	136.9	136.9	NUM
eurjchem-1701	98	38	,	,	PUNCT
eurjchem-1701	98	39	129.7	129.7	NUM
eurjchem-1701	98	40	,	,	PUNCT
eurjchem-1701	98	41	129.4	129.4	NUM
eurjchem-1701	98	42	,	,	PUNCT
eurjchem-1701	98	43	128.8	128.8	NUM
eurjchem-1701	98	44	,	,	PUNCT
eurjchem-1701	98	45	128.2	128.2	NUM
eurjchem-1701	98	46	,	,	PUNCT
eurjchem-1701	98	47	127.1	127.1	NUM
eurjchem-1701	98	48	,	,	PUNCT
eurjchem-1701	98	49	122.1	122.1	NUM
eurjchem-1701	98	50	,	,	PUNCT
eurjchem-1701	98	51	121.2	121.2	NUM
eurjchem-1701	98	52	,	,	PUNCT
eurjchem-1701	98	53	(	(	PUNCT
eurjchem-1701	98	54	ar	ar	NOUN
eurjchem-1701	98	55	-	-	NOUN
eurjchem-1701	98	56	c	c	NOUN
eurjchem-1701	98	57	)	)	PUNCT
eurjchem-1701	98	58	,	,	PUNCT
eurjchem-1701	98	59	23.8	23.8	NUM
eurjchem-1701	98	60	(	(	PUNCT
eurjchem-1701	98	61	1c	1c	NOUN
eurjchem-1701	98	62	,	,	PUNCT
eurjchem-1701	98	63	ch2	ch2	PROPN
eurjchem-1701	98	64	)	)	PUNCT
eurjchem-1701	98	65	.	.	PUNCT
eurjchem-1701	99	1	ms	ms	NOUN
eurjchem-1701	99	2	(	(	PUNCT
eurjchem-1701	99	3	ei	ei	PROPN
eurjchem-1701	99	4	,	,	PUNCT
eurjchem-1701	99	5	m	m	PROPN
eurjchem-1701	99	6	/	/	SYM
eurjchem-1701	99	7	z	z	PROPN
eurjchem-1701	99	8	(	(	PUNCT
eurjchem-1701	99	9	%	%	NOUN
eurjchem-1701	99	10	)	)	PUNCT
eurjchem-1701	99	11	):	):	PUNCT
eurjchem-1701	99	12	357	357	NUM
eurjchem-1701	99	13	(	(	PUNCT
eurjchem-1701	99	14	m+	m+	NUM
eurjchem-1701	99	15	,	,	PUNCT
eurjchem-1701	99	16	20	20	NUM
eurjchem-1701	99	17	)	)	PUNCT
eurjchem-1701	99	18	,	,	PUNCT
eurjchem-1701	99	19	259	259	NUM
eurjchem-1701	99	20	(	(	PUNCT
eurjchem-1701	99	21	100	100	NUM
eurjchem-1701	99	22	)	)	PUNCT
eurjchem-1701	99	23	,	,	PUNCT
eurjchem-1701	99	24	215	215	NUM
eurjchem-1701	99	25	(	(	PUNCT
eurjchem-1701	99	26	10	10	NUM
eurjchem-1701	99	27	)	)	PUNCT
eurjchem-1701	99	28	,	,	PUNCT
eurjchem-1701	99	29	91	91	NUM
eurjchem-1701	99	30	(	(	PUNCT
eurjchem-1701	99	31	25	25	NUM
eurjchem-1701	99	32	)	)	PUNCT
eurjchem-1701	99	33	.	.	PUNCT
eurjchem-1701	100	1	anal	anal	PROPN
eurjchem-1701	100	2	.	.	PUNCT
eurjchem-1701	100	3	calcd	calcd	NOUN
eurjchem-1701	100	4	.	.	PUNCT
eurjchem-1701	101	1	for	for	ADP
eurjchem-1701	101	2	c16h11n3o3s2	c16h11n3o3s2	NOUN
eurjchem-1701	101	3	:	:	PUNCT
eurjchem-1701	101	4	c	c	X
eurjchem-1701	101	5	,	,	PUNCT
eurjchem-1701	101	6	53.77	53.77	NUM
eurjchem-1701	101	7	;	;	PUNCT
eurjchem-1701	101	8	h	h	NOUN
eurjchem-1701	101	9	,	,	PUNCT
eurjchem-1701	101	10	3.10	3.10	NUM
eurjchem-1701	101	11	;	;	PUNCT
eurjchem-1701	101	12	n	n	CCONJ
eurjchem-1701	101	13	,	,	PUNCT
eurjchem-1701	101	14	11.76	11.76	NUM
eurjchem-1701	101	15	.	.	PUNCT
eurjchem-1701	102	1	found	find	VERB
eurjchem-1701	102	2	:	:	PUNCT
eurjchem-1701	103	1	c	c	X
eurjchem-1701	103	2	,	,	PUNCT
eurjchem-1701	103	3	53.68	53.68	NUM
eurjchem-1701	103	4	;	;	PUNCT
eurjchem-1701	104	1	h	h	NOUN
eurjchem-1701	104	2	,	,	PUNCT
eurjchem-1701	104	3	2.99	2.99	NUM
eurjchem-1701	104	4	;	;	PUNCT
eurjchem-1701	104	5	n	n	CCONJ
eurjchem-1701	104	6	,	,	PUNCT
eurjchem-1701	104	7	11.70	11.70	NUM
eurjchem-1701	104	8	%	%	NOUN
eurjchem-1701	104	9	.	.	PUNCT
eurjchem-1701	105	1	2.3.6	2.3.6	NUM
eurjchem-1701	105	2	.	.	X
eurjchem-1701	105	3	synthesis	synthesis	NOUN
eurjchem-1701	105	4	of	of	ADP
eurjchem-1701	105	5	n-(5	n-(5	PROPN
eurjchem-1701	105	6	-	-	PUNCT
eurjchem-1701	105	7	hydroxy-3	hydroxy-3	PROPN
eurjchem-1701	105	8	-	-	PUNCT
eurjchem-1701	105	9	phenyl-3,6	phenyl-3,6	NOUN
eurjchem-1701	105	10	-	-	PUNCT
eurjchem-1701	105	11	dihydro-2h1,3,4	dihydro-2h1,3,4	NOUN
eurjchem-1701	105	12	-	-	PUNCT
eurjchem-1701	105	13	thiadiazin-2	thiadiazin-2	NUM
eurjchem-1701	105	14	-	-	PUNCT
eurjchem-1701	105	15	ylidene)thiophene-2	ylidene)thiophene-2	NOUN
eurjchem-1701	105	16	-	-	PUNCT
eurjchem-1701	105	17	carboxamide	carboxamide	NOUN
eurjchem-1701	105	18	(	(	PUNCT
eurjchem-1701	105	19	7	7	X
eurjchem-1701	105	20	)	)	PUNCT
eurjchem-1701	105	21	a	a	DET
eurjchem-1701	105	22	mixture	mixture	NOUN
eurjchem-1701	105	23	of	of	ADP
eurjchem-1701	105	24	n-(1	n-(1	NOUN
eurjchem-1701	105	25	-	-	PUNCT
eurjchem-1701	105	26	phenylhydrazinecarbonothioyl)thiophene	phenylhydrazinecarbonothioyl)thiophene	ADJ
eurjchem-1701	105	27	2018	2018	NUM
eurjchem-1701	105	28	–	–	PUNCT
eurjchem-1701	105	29	european	european	ADJ
eurjchem-1701	105	30	journal	journal	NOUN
eurjchem-1701	105	31	of	of	ADP
eurjchem-1701	105	32	chemistry	chemistry	NOUN
eurjchem-1701	105	33	–	–	PUNCT
eurjchem-1701	105	34	cc	cc	NOUN
eurjchem-1701	105	35	by	by	ADP
eurjchem-1701	105	36	nc	nc	PROPN
eurjchem-1701	105	37	–	–	PUNCT
eurjchem-1701	105	38	doi	doi	NOUN
eurjchem-1701	105	39	:	:	PUNCT
eurjchem-1701	105	40	10.5155	10.5155	NUM
eurjchem-1701	105	41	/	/	SYM
eurjchem-1701	105	42	eurjchem.9.2.99	eurjchem.9.2.99	NUM
eurjchem-1701	105	43	-	-	PUNCT
eurjchem-1701	105	44	106.1701	106.1701	NUM
eurjchem-1701	105	45	haggam	haggam	NOUN
eurjchem-1701	105	46	et	et	PROPN
eurjchem-1701	105	47	al	al	PROPN
eurjchem-1701	105	48	.	.	PUNCT
eurjchem-1701	105	49	/	/	SYM
eurjchem-1701	105	50	european	european	PROPN
eurjchem-1701	105	51	journal	journal	PROPN
eurjchem-1701	105	52	of	of	ADP
eurjchem-1701	105	53	chemistry	chemistry	NOUN
eurjchem-1701	105	54	9	9	NUM
eurjchem-1701	105	55	(	(	PUNCT
eurjchem-1701	105	56	2	2	NUM
eurjchem-1701	105	57	)	)	PUNCT
eurjchem-1701	105	58	(	(	PUNCT
eurjchem-1701	105	59	2018	2018	NUM
eurjchem-1701	105	60	)	)	PUNCT
eurjchem-1701	105	61	99	99	NUM
eurjchem-1701	105	62	-	-	SYM
eurjchem-1701	105	63	106	106	NUM
eurjchem-1701	105	64	101	101	NUM
eurjchem-1701	105	65	s	s	NOUN
eurjchem-1701	105	66	1	1	NUM
eurjchem-1701	105	67	4	4	NUM
eurjchem-1701	105	68	dioxane	dioxane	NOUN
eurjchem-1701	105	69	/	/	SYM
eurjchem-1701	105	70	h2o	h2o	PROPN
eurjchem-1701	105	71	(	(	PUNCT
eurjchem-1701	105	72	1:1	1:1	NUM
eurjchem-1701	105	73	)	)	PUNCT
eurjchem-1701	105	74	stirring	stirring	NOUN
eurjchem-1701	105	75	/	/	SYM
eurjchem-1701	105	76	r.t	r.t	PROPN
eurjchem-1701	105	77	.	.	PROPN
eurjchem-1701	105	78	/	/	SYM
eurjchem-1701	105	79	1	1	NUM
eurjchem-1701	105	80	h	h	NOUN
eurjchem-1701	105	81	33	33	NUM
eurjchem-1701	105	82	%	%	NOUN
eurjchem-1701	105	83	s	s	PART
eurjchem-1701	105	84	n	n	NOUN
eurjchem-1701	105	85	o	o	NOUN
eurjchem-1701	105	86	n	n	CCONJ
eurjchem-1701	105	87	s	s	NOUN
eurjchem-1701	105	88	n	n	PRON
eurjchem-1701	105	89	h	h	NOUN
eurjchem-1701	105	90	n	n	NOUN
eurjchem-1701	105	91	h	h	NOUN
eurjchem-1701	105	92	2	2	NUM
eurjchem-1701	105	93	3	3	NUM
eurjchem-1701	105	94	o	o	NOUN
eurjchem-1701	105	95	h	h	NOUN
eurjchem-1701	106	1	n	n	NOUN
eurjchem-1701	106	2	h	h	NOUN
eurjchem-1701	107	1	n	n	NOUN
eurjchem-1701	107	2	s	s	NOUN
eurjchem-1701	107	3	h	h	NOUN
eurjchem-1701	107	4	n	n	ADV
eurjchem-1701	107	5	o	o	X
eurjchem-1701	108	1	nh2s	nh2s	INTJ
eurjchem-1701	108	2	o	o	INTJ
eurjchem-1701	108	3	h	h	NOUN
eurjchem-1701	109	1	n	n	NOUN
eurjchem-1701	109	2	h	h	NOUN
eurjchem-1701	109	3	n	n	CCONJ
eurjchem-1701	110	1	n	n	NOUN
eurjchem-1701	110	2	h	h	NOUN
eurjchem-1701	110	3	s	s	PART
eurjchem-1701	110	4	ph	ph	PROPN
eurjchem-1701	110	5	s	s	NOUN
eurjchem-1701	110	6	o	o	NOUN
eurjchem-1701	110	7	n	n	ADP
eurjchem-1701	110	8	c	c	NOUN
eurjchem-1701	110	9	s	s	NOUN
eurjchem-1701	110	10	s	s	X
eurjchem-1701	110	11	n	n	PRON
eurjchem-1701	110	12	nh	nh	PROPN
eurjchem-1701	110	13	n	n	CCONJ
eurjchem-1701	110	14	ph	ph	PROPN
eurjchem-1701	110	15	s	s	PART
eurjchem-1701	110	16	hcl	hcl	PROPN
eurjchem-1701	110	17	h2o	h2o	PROPN
eurjchem-1701	110	18	h2n	h2n	PROPN
eurjchem-1701	111	1	n	n	PRON
eurjchem-1701	111	2	h	h	NOUN
eurjchem-1701	111	3	nh3	nh3	NOUN
eurjchem-1701	111	4	cl	cl	NOUN
eurjchem-1701	111	5	o	o	NOUN
eurjchem-1701	111	6	h2n	h2n	PROPN
eurjchem-1701	112	1	n	n	PRON
eurjchem-1701	112	2	h	h	NOUN
eurjchem-1701	112	3	ph	ph	ADJ
eurjchem-1701	112	4	dioxane	dioxane	NOUN
eurjchem-1701	112	5	/	/	SYM
eurjchem-1701	112	6	reflux	reflux	NOUN
eurjchem-1701	112	7	2	2	NUM
eurjchem-1701	112	8	h	h	NOUN
eurjchem-1701	112	9	63	63	NUM
eurjchem-1701	112	10	%	%	NOUN
eurjchem-1701	112	11	naoet	naoet	ADJ
eurjchem-1701	112	12	/	/	SYM
eurjchem-1701	112	13	etoh	etoh	PROPN
eurjchem-1701	112	14	reflux	reflux	NOUN
eurjchem-1701	112	15	2	2	NUM
eurjchem-1701	112	16	h	h	NOUN
eurjchem-1701	112	17	89	89	NUM
eurjchem-1701	112	18	%	%	NOUN
eurjchem-1701	112	19	h	h	NOUN
eurjchem-1701	112	20	scheme	scheme	NOUN
eurjchem-1701	112	21	1	1	NUM
eurjchem-1701	112	22	2	2	NUM
eurjchem-1701	112	23	-	-	PUNCT
eurjchem-1701	112	24	carboxamide	carboxamide	NOUN
eurjchem-1701	112	25	hydrochloride	hydrochloride	NOUN
eurjchem-1701	112	26	(	(	PUNCT
eurjchem-1701	112	27	5	5	NUM
eurjchem-1701	112	28	)	)	PUNCT
eurjchem-1701	112	29	(	(	PUNCT
eurjchem-1701	112	30	1.50	1.50	NUM
eurjchem-1701	112	31	mol	mol	NOUN
eurjchem-1701	112	32	)	)	PUNCT
eurjchem-1701	112	33	,	,	PUNCT
eurjchem-1701	112	34	ethyl	ethyl	PROPN
eurjchem-1701	112	35	chloroacetate	chloroacetate	NOUN
eurjchem-1701	112	36	(	(	PUNCT
eurjchem-1701	112	37	1.50	1.50	NUM
eurjchem-1701	112	38	mol	mol	NOUN
eurjchem-1701	112	39	)	)	PUNCT
eurjchem-1701	112	40	and	and	CCONJ
eurjchem-1701	112	41	triethyl	triethyl	PROPN
eurjchem-1701	112	42	amine	amine	PROPN
eurjchem-1701	112	43	(	(	PUNCT
eurjchem-1701	112	44	1.50	1.50	NUM
eurjchem-1701	112	45	mole	mole	NOUN
eurjchem-1701	112	46	)	)	PUNCT
eurjchem-1701	112	47	in	in	ADP
eurjchem-1701	112	48	ethanol	ethanol	NOUN
eurjchem-1701	112	49	(	(	PUNCT
eurjchem-1701	112	50	20	20	NUM
eurjchem-1701	112	51	ml	ml	NOUN
eurjchem-1701	112	52	)	)	PUNCT
eurjchem-1701	112	53	was	be	AUX
eurjchem-1701	112	54	heated	heat	VERB
eurjchem-1701	112	55	under	under	ADP
eurjchem-1701	112	56	reflux	reflux	NOUN
eurjchem-1701	112	57	for	for	ADP
eurjchem-1701	112	58	6	6	NUM
eurjchem-1701	112	59	h.	h.	NOUN
eurjchem-1701	112	60	the	the	DET
eurjchem-1701	112	61	reaction	reaction	NOUN
eurjchem-1701	112	62	mixture	mixture	NOUN
eurjchem-1701	112	63	was	be	AUX
eurjchem-1701	112	64	neutralized	neutralize	VERB
eurjchem-1701	112	65	by	by	ADP
eurjchem-1701	112	66	10	10	NUM
eurjchem-1701	112	67	%	%	NOUN
eurjchem-1701	112	68	hcl	hcl	PROPN
eurjchem-1701	112	69	.	.	PUNCT
eurjchem-1701	113	1	the	the	DET
eurjchem-1701	113	2	formed	form	VERB
eurjchem-1701	113	3	precipitate	precipitate	NOUN
eurjchem-1701	113	4	was	be	AUX
eurjchem-1701	113	5	filtered	filter	VERB
eurjchem-1701	113	6	off	off	ADP
eurjchem-1701	113	7	,	,	PUNCT
eurjchem-1701	113	8	dried	dry	VERB
eurjchem-1701	113	9	and	and	CCONJ
eurjchem-1701	113	10	crystallized	crystallize	VERB
eurjchem-1701	113	11	from	from	ADP
eurjchem-1701	113	12	ethanol	ethanol	NOUN
eurjchem-1701	113	13	to	to	PART
eurjchem-1701	113	14	give	give	VERB
eurjchem-1701	113	15	compound	compound	NOUN
eurjchem-1701	113	16	7	7	NUM
eurjchem-1701	113	17	(	(	PUNCT
eurjchem-1701	113	18	scheme	scheme	NOUN
eurjchem-1701	113	19	2	2	NUM
eurjchem-1701	113	20	)	)	PUNCT
eurjchem-1701	113	21	.	.	PUNCT
eurjchem-1701	114	1	color	color	NOUN
eurjchem-1701	114	2	:	:	PUNCT
eurjchem-1701	114	3	white	white	ADJ
eurjchem-1701	114	4	.	.	PUNCT
eurjchem-1701	115	1	yield	yield	NOUN
eurjchem-1701	115	2	:	:	PUNCT
eurjchem-1701	115	3	79	79	NUM
eurjchem-1701	115	4	%	%	NOUN
eurjchem-1701	115	5	.	.	PUNCT
eurjchem-1701	116	1	m.p	m.p	AUX
eurjchem-1701	116	2	.	.	PROPN
eurjchem-1701	116	3	:	:	PUNCT
eurjchem-1701	116	4	280281	280281	NUM
eurjchem-1701	116	5	°	°	SYM
eurjchem-1701	116	6	c	c	NOUN
eurjchem-1701	116	7	.	.	PUNCT
eurjchem-1701	116	8	ft	ft	PROPN
eurjchem-1701	116	9	-	-	PUNCT
eurjchem-1701	116	10	ir	ir	PROPN
eurjchem-1701	116	11	(	(	PUNCT
eurjchem-1701	116	12	kbr	kbr	PROPN
eurjchem-1701	116	13	,	,	PUNCT
eurjchem-1701	116	14	ν	ν	PROPN
eurjchem-1701	116	15	,	,	PUNCT
eurjchem-1701	116	16	cm-1	cm-1	NUM
eurjchem-1701	116	17	):	):	PUNCT
eurjchem-1701	116	18	3631	3631	NUM
eurjchem-1701	116	19	(	(	PUNCT
eurjchem-1701	116	20	oh	oh	INTJ
eurjchem-1701	116	21	)	)	PUNCT
eurjchem-1701	116	22	,	,	PUNCT
eurjchem-1701	116	23	3117	3117	NUM
eurjchem-1701	116	24	(	(	PUNCT
eurjchem-1701	116	25	ch	ch	NOUN
eurjchem-1701	116	26	arom	arom	NOUN
eurjchem-1701	116	27	.	.	PUNCT
eurjchem-1701	116	28	)	)	PUNCT
eurjchem-1701	116	29	,	,	PUNCT
eurjchem-1701	116	30	1667	1667	NUM
eurjchem-1701	116	31	(	(	PUNCT
eurjchem-1701	116	32	c	c	NOUN
eurjchem-1701	116	33	=	=	NOUN
eurjchem-1701	116	34	o	o	NOUN
eurjchem-1701	116	35	)	)	PUNCT
eurjchem-1701	116	36	(	(	PUNCT
eurjchem-1701	116	37	amide	amide	NOUN
eurjchem-1701	116	38	)	)	PUNCT
eurjchem-1701	116	39	,	,	PUNCT
eurjchem-1701	116	40	1631	1631	NUM
eurjchem-1701	116	41	(	(	PUNCT
eurjchem-1701	116	42	c	c	NOUN
eurjchem-1701	116	43	=	=	SYM
eurjchem-1701	116	44	n	n	CCONJ
eurjchem-1701	116	45	)	)	PUNCT
eurjchem-1701	116	46	1220	1220	NUM
eurjchem-1701	116	47	(	(	PUNCT
eurjchem-1701	116	48	c	c	NOUN
eurjchem-1701	116	49	-	-	PUNCT
eurjchem-1701	116	50	o	o	NOUN
eurjchem-1701	116	51	)	)	PUNCT
eurjchem-1701	116	52	.	.	PUNCT
eurjchem-1701	117	1	1h	1h	NUM
eurjchem-1701	117	2	nmr	nmr	NOUN
eurjchem-1701	117	3	(	(	PUNCT
eurjchem-1701	117	4	300	300	NUM
eurjchem-1701	117	5	mhz	mhz	NOUN
eurjchem-1701	117	6	,	,	PUNCT
eurjchem-1701	117	7	dmso	dmso	NOUN
eurjchem-1701	117	8	-	-	NOUN
eurjchem-1701	117	9	d6	d6	NOUN
eurjchem-1701	117	10	,	,	PUNCT
eurjchem-1701	117	11	δ	δ	PROPN
eurjchem-1701	117	12	,	,	PUNCT
eurjchem-1701	117	13	ppm	ppm	NUM
eurjchem-1701	117	14	):	):	PUNCT
eurjchem-1701	117	15	2.23	2.23	NUM
eurjchem-1701	117	16	(	(	PUNCT
eurjchem-1701	117	17	s	s	PROPN
eurjchem-1701	117	18	,	,	PUNCT
eurjchem-1701	117	19	2h	2h	NUM
eurjchem-1701	117	20	,	,	PUNCT
eurjchem-1701	117	21	ch2	ch2	PROPN
eurjchem-1701	117	22	)	)	PUNCT
eurjchem-1701	117	23	,	,	PUNCT
eurjchem-1701	117	24	8.28	8.28	NUM
eurjchem-1701	117	25	-	-	SYM
eurjchem-1701	117	26	7.15	7.15	NUM
eurjchem-1701	117	27	(	(	PUNCT
eurjchem-1701	117	28	m	m	PROPN
eurjchem-1701	117	29	,	,	PUNCT
eurjchem-1701	117	30	8h	8h	NUM
eurjchem-1701	117	31	,	,	PUNCT
eurjchem-1701	117	32	arh	arh	PROPN
eurjchem-1701	117	33	’s	’s	PART
eurjchem-1701	117	34	+	+	NUM
eurjchem-1701	117	35	thiophene	thiophene	NOUN
eurjchem-1701	117	36	protons	proton	NOUN
eurjchem-1701	117	37	)	)	PUNCT
eurjchem-1701	117	38	,	,	PUNCT
eurjchem-1701	117	39	12.95	12.95	NUM
eurjchem-1701	117	40	(	(	PUNCT
eurjchem-1701	117	41	s	s	PROPN
eurjchem-1701	117	42	,	,	PUNCT
eurjchem-1701	117	43	1h	1h	NUM
eurjchem-1701	117	44	,	,	PUNCT
eurjchem-1701	117	45	d2o	d2o	NOUN
eurjchem-1701	117	46	exchangeable	exchangeable	ADJ
eurjchem-1701	117	47	,	,	PUNCT
eurjchem-1701	117	48	oh	oh	INTJ
eurjchem-1701	117	49	)	)	PUNCT
eurjchem-1701	117	50	.	.	PUNCT
eurjchem-1701	118	1	13c	13c	NOUN
eurjchem-1701	118	2	nmr	nmr	NOUN
eurjchem-1701	118	3	(	(	PUNCT
eurjchem-1701	118	4	75.4	75.4	NUM
eurjchem-1701	118	5	mhz	mhz	NOUN
eurjchem-1701	118	6	,	,	PUNCT
eurjchem-1701	118	7	dmso	dmso	NOUN
eurjchem-1701	118	8	-	-	NOUN
eurjchem-1701	118	9	d6	d6	NOUN
eurjchem-1701	118	10	,	,	PUNCT
eurjchem-1701	118	11	δ	δ	PROPN
eurjchem-1701	118	12	,	,	PUNCT
eurjchem-1701	118	13	ppm	ppm	NOUN
eurjchem-1701	118	14	):	):	PUNCT
eurjchem-1701	118	15	165.8	165.8	NUM
eurjchem-1701	118	16	(	(	PUNCT
eurjchem-1701	118	17	1c	1c	NOUN
eurjchem-1701	118	18	,	,	PUNCT
eurjchem-1701	118	19	c	c	NOUN
eurjchem-1701	118	20	=	=	SYM
eurjchem-1701	118	21	o	o	NOUN
eurjchem-1701	118	22	)	)	PUNCT
eurjchem-1701	118	23	,	,	PUNCT
eurjchem-1701	118	24	159.1	159.1	NUM
eurjchem-1701	118	25	,	,	PUNCT
eurjchem-1701	118	26	156.4	156.4	NUM
eurjchem-1701	118	27	(	(	PUNCT
eurjchem-1701	118	28	2c	2c	NUM
eurjchem-1701	118	29	,	,	PUNCT
eurjchem-1701	118	30	c	c	NOUN
eurjchem-1701	118	31	=	=	SYM
eurjchem-1701	118	32	n	n	NUM
eurjchem-1701	118	33	)	)	PUNCT
eurjchem-1701	118	34	,	,	PUNCT
eurjchem-1701	118	35	136.1	136.1	NUM
eurjchem-1701	118	36	,	,	PUNCT
eurjchem-1701	118	37	129.2	129.2	NUM
eurjchem-1701	118	38	,	,	PUNCT
eurjchem-1701	118	39	128.8	128.8	NUM
eurjchem-1701	118	40	,	,	PUNCT
eurjchem-1701	118	41	128.4	128.4	NUM
eurjchem-1701	118	42	,	,	PUNCT
eurjchem-1701	118	43	127.9	127.9	NUM
eurjchem-1701	118	44	,	,	PUNCT
eurjchem-1701	118	45	127.0	127.0	NUM
eurjchem-1701	118	46	,	,	PUNCT
eurjchem-1701	118	47	123.1	123.1	NUM
eurjchem-1701	118	48	,	,	PUNCT
eurjchem-1701	118	49	121.8	121.8	NUM
eurjchem-1701	118	50	(	(	PUNCT
eurjchem-1701	118	51	ar	ar	NOUN
eurjchem-1701	118	52	-	-	NOUN
eurjchem-1701	118	53	c	c	NOUN
eurjchem-1701	118	54	)	)	PUNCT
eurjchem-1701	118	55	,	,	PUNCT
eurjchem-1701	118	56	34.3	34.3	NUM
eurjchem-1701	118	57	(	(	PUNCT
eurjchem-1701	118	58	1c	1c	NOUN
eurjchem-1701	118	59	,	,	PUNCT
eurjchem-1701	118	60	sch2	sch2	PROPN
eurjchem-1701	118	61	)	)	PUNCT
eurjchem-1701	118	62	.	.	PUNCT
eurjchem-1701	119	1	ms	ms	NOUN
eurjchem-1701	119	2	(	(	PUNCT
eurjchem-1701	119	3	ei	ei	PROPN
eurjchem-1701	119	4	,	,	PUNCT
eurjchem-1701	119	5	m	m	PROPN
eurjchem-1701	119	6	/	/	SYM
eurjchem-1701	119	7	z	z	PROPN
eurjchem-1701	119	8	(	(	PUNCT
eurjchem-1701	119	9	%	%	NOUN
eurjchem-1701	119	10	)	)	PUNCT
eurjchem-1701	119	11	):	):	PUNCT
eurjchem-1701	119	12	317(m+	317(m+	NUM
eurjchem-1701	119	13	,	,	PUNCT
eurjchem-1701	119	14	100	100	NUM
eurjchem-1701	119	15	)	)	PUNCT
eurjchem-1701	119	16	,	,	PUNCT
eurjchem-1701	119	17	271	271	NUM
eurjchem-1701	119	18	(	(	PUNCT
eurjchem-1701	119	19	20	20	NUM
eurjchem-1701	119	20	)	)	PUNCT
eurjchem-1701	119	21	,	,	PUNCT
eurjchem-1701	119	22	200	200	NUM
eurjchem-1701	119	23	(	(	PUNCT
eurjchem-1701	119	24	30	30	NUM
eurjchem-1701	119	25	)	)	PUNCT
eurjchem-1701	119	26	,	,	PUNCT
eurjchem-1701	119	27	110	110	NUM
eurjchem-1701	119	28	(	(	PUNCT
eurjchem-1701	119	29	30	30	NUM
eurjchem-1701	119	30	)	)	PUNCT
eurjchem-1701	119	31	,	,	PUNCT
eurjchem-1701	119	32	91	91	NUM
eurjchem-1701	119	33	(	(	PUNCT
eurjchem-1701	119	34	10	10	NUM
eurjchem-1701	119	35	)	)	PUNCT
eurjchem-1701	119	36	,	,	PUNCT
eurjchem-1701	119	37	77	77	NUM
eurjchem-1701	119	38	(	(	PUNCT
eurjchem-1701	119	39	50	50	NUM
eurjchem-1701	119	40	)	)	PUNCT
eurjchem-1701	119	41	.	.	PUNCT
eurjchem-1701	120	1	anal	anal	PROPN
eurjchem-1701	120	2	.	.	PUNCT
eurjchem-1701	120	3	calcd	calcd	NOUN
eurjchem-1701	120	4	.	.	PUNCT
eurjchem-1701	121	1	for	for	ADP
eurjchem-1701	121	2	c14h11n3o2s2	c14h11n3o2s2	NOUN
eurjchem-1701	121	3	:	:	PUNCT
eurjchem-1701	121	4	c	c	X
eurjchem-1701	121	5	,	,	PUNCT
eurjchem-1701	121	6	52.98	52.98	NUM
eurjchem-1701	121	7	;	;	PUNCT
eurjchem-1701	121	8	h	h	NOUN
eurjchem-1701	121	9	,	,	PUNCT
eurjchem-1701	121	10	3.49	3.49	NUM
eurjchem-1701	121	11	;	;	PUNCT
eurjchem-1701	121	12	n	n	CCONJ
eurjchem-1701	121	13	,	,	PUNCT
eurjchem-1701	121	14	13.24	13.24	NUM
eurjchem-1701	121	15	.	.	PUNCT
eurjchem-1701	121	16	found	find	VERB
eurjchem-1701	121	17	:	:	PUNCT
eurjchem-1701	122	1	c	c	X
eurjchem-1701	122	2	,	,	PUNCT
eurjchem-1701	122	3	52.93	52.93	NUM
eurjchem-1701	122	4	;	;	PUNCT
eurjchem-1701	123	1	h	h	NOUN
eurjchem-1701	123	2	,	,	PUNCT
eurjchem-1701	123	3	3.40	3.40	NUM
eurjchem-1701	123	4	;	;	PUNCT
eurjchem-1701	123	5	n	n	CCONJ
eurjchem-1701	123	6	,	,	PUNCT
eurjchem-1701	123	7	13.16	13.16	NUM
eurjchem-1701	123	8	%	%	NOUN
eurjchem-1701	123	9	.	.	PUNCT
eurjchem-1701	124	1	2.3.7	2.3.7	X
eurjchem-1701	124	2	.	.	PUNCT
eurjchem-1701	125	1	synthesis	synthesis	NOUN
eurjchem-1701	125	2	of	of	ADP
eurjchem-1701	125	3	1,2	1,2	NUM
eurjchem-1701	125	4	-	-	PUNCT
eurjchem-1701	125	5	dihydro-2	dihydro-2	NUM
eurjchem-1701	125	6	-	-	PUNCT
eurjchem-1701	125	7	phenyl-5-(thiophen-2	phenyl-5-(thiophen-2	NOUN
eurjchem-1701	125	8	-	-	PUNCT
eurjchem-1701	125	9	yl)1,2,4	yl)1,2,4	NOUN
eurjchem-1701	125	10	-	-	PUNCT
eurjchem-1701	125	11	triazole-3	triazole-3	NOUN
eurjchem-1701	125	12	-	-	PUNCT
eurjchem-1701	125	13	thione	thione	NOUN
eurjchem-1701	125	14	(	(	PUNCT
eurjchem-1701	125	15	8)	8)	NUM
eurjchem-1701	125	16	a	a	DET
eurjchem-1701	125	17	mixture	mixture	NOUN
eurjchem-1701	125	18	of	of	ADP
eurjchem-1701	125	19	n-(1	n-(1	NOUN
eurjchem-1701	125	20	-	-	PUNCT
eurjchem-1701	125	21	phenylhydrazinecarbonothioyl)thiophene-2	phenylhydrazinecarbonothioyl)thiophene-2	PRON
eurjchem-1701	125	22	-	-	PUNCT
eurjchem-1701	125	23	carboxamide	carboxamide	NOUN
eurjchem-1701	125	24	hydrochloride	hydrochloride	NOUN
eurjchem-1701	125	25	(	(	PUNCT
eurjchem-1701	125	26	5	5	NUM
eurjchem-1701	125	27	)	)	PUNCT
eurjchem-1701	125	28	(	(	PUNCT
eurjchem-1701	125	29	1.50	1.50	NUM
eurjchem-1701	125	30	mol	mol	NOUN
eurjchem-1701	125	31	)	)	PUNCT
eurjchem-1701	125	32	and	and	CCONJ
eurjchem-1701	125	33	sodium	sodium	NOUN
eurjchem-1701	125	34	ethoxide	ethoxide	NOUN
eurjchem-1701	125	35	(	(	PUNCT
eurjchem-1701	125	36	1.50	1.50	NUM
eurjchem-1701	125	37	mol	mol	NOUN
eurjchem-1701	125	38	)	)	PUNCT
eurjchem-1701	125	39	in	in	ADP
eurjchem-1701	125	40	ethanol	ethanol	NOUN
eurjchem-1701	125	41	(	(	PUNCT
eurjchem-1701	125	42	20	20	NUM
eurjchem-1701	125	43	ml	ml	NOUN
eurjchem-1701	125	44	)	)	PUNCT
eurjchem-1701	125	45	was	be	AUX
eurjchem-1701	125	46	heated	heat	VERB
eurjchem-1701	125	47	under	under	ADP
eurjchem-1701	125	48	reflux	reflux	NOUN
eurjchem-1701	125	49	for	for	ADP
eurjchem-1701	125	50	2	2	NUM
eurjchem-1701	125	51	h.	h.	NOUN
eurjchem-1701	125	52	the	the	DET
eurjchem-1701	125	53	reaction	reaction	NOUN
eurjchem-1701	125	54	mixture	mixture	NOUN
eurjchem-1701	125	55	was	be	AUX
eurjchem-1701	125	56	neutralized	neutralize	VERB
eurjchem-1701	125	57	by	by	ADP
eurjchem-1701	125	58	10	10	NUM
eurjchem-1701	125	59	%	%	NOUN
eurjchem-1701	125	60	hcl	hcl	PROPN
eurjchem-1701	125	61	.	.	PUNCT
eurjchem-1701	126	1	the	the	DET
eurjchem-1701	126	2	formed	form	VERB
eurjchem-1701	126	3	precipitate	precipitate	NOUN
eurjchem-1701	126	4	was	be	AUX
eurjchem-1701	126	5	filtered	filter	VERB
eurjchem-1701	126	6	off	off	ADP
eurjchem-1701	126	7	,	,	PUNCT
eurjchem-1701	126	8	dried	dry	VERB
eurjchem-1701	126	9	and	and	CCONJ
eurjchem-1701	126	10	crystallized	crystallize	VERB
eurjchem-1701	126	11	from	from	ADP
eurjchem-1701	126	12	ethanol	ethanol	NOUN
eurjchem-1701	126	13	to	to	PART
eurjchem-1701	126	14	give	give	VERB
eurjchem-1701	126	15	compound	compound	NOUN
eurjchem-1701	126	16	8	8	NUM
eurjchem-1701	126	17	(	(	PUNCT
eurjchem-1701	126	18	scheme	scheme	NOUN
eurjchem-1701	126	19	2	2	NUM
eurjchem-1701	126	20	)	)	PUNCT
eurjchem-1701	126	21	.	.	PUNCT
eurjchem-1701	127	1	color	color	NOUN
eurjchem-1701	127	2	:	:	PUNCT
eurjchem-1701	127	3	pale	pale	ADJ
eurjchem-1701	127	4	white	white	ADJ
eurjchem-1701	127	5	.	.	PUNCT
eurjchem-1701	128	1	yield	yield	NOUN
eurjchem-1701	128	2	:	:	PUNCT
eurjchem-1701	128	3	95	95	NUM
eurjchem-1701	128	4	%	%	NOUN
eurjchem-1701	128	5	.	.	PUNCT
eurjchem-1701	129	1	m.p	m.p	PROPN
eurjchem-1701	129	2	.	.	PROPN
eurjchem-1701	129	3	:	:	PUNCT
eurjchem-1701	130	1	290	290	NUM
eurjchem-1701	130	2	-	-	SYM
eurjchem-1701	130	3	291	291	NUM
eurjchem-1701	130	4	°	°	NOUN
eurjchem-1701	130	5	c	c	NOUN
eurjchem-1701	130	6	.	.	PUNCT
eurjchem-1701	131	1	ft	ft	PROPN
eurjchem-1701	131	2	-	-	PUNCT
eurjchem-1701	131	3	ir	ir	PROPN
eurjchem-1701	131	4	(	(	PUNCT
eurjchem-1701	131	5	kbr	kbr	PROPN
eurjchem-1701	131	6	,	,	PUNCT
eurjchem-1701	131	7	ν	ν	PROPN
eurjchem-1701	131	8	,	,	PUNCT
eurjchem-1701	131	9	cm-1	cm-1	NUM
eurjchem-1701	131	10	):	):	PUNCT
eurjchem-1701	131	11	3424	3424	NUM
eurjchem-1701	131	12	(	(	PUNCT
eurjchem-1701	131	13	nh	nh	NOUN
eurjchem-1701	131	14	)	)	PUNCT
eurjchem-1701	131	15	,	,	PUNCT
eurjchem-1701	131	16	1635	1635	NUM
eurjchem-1701	131	17	(	(	PUNCT
eurjchem-1701	131	18	c	c	NOUN
eurjchem-1701	131	19	=	=	SYM
eurjchem-1701	131	20	n	n	NUM
eurjchem-1701	131	21	)	)	PUNCT
eurjchem-1701	131	22	,	,	PUNCT
eurjchem-1701	131	23	1597	1597	NUM
eurjchem-1701	131	24	(	(	PUNCT
eurjchem-1701	131	25	c	c	NOUN
eurjchem-1701	131	26	=	=	SYM
eurjchem-1701	131	27	c	c	NOUN
eurjchem-1701	131	28	)	)	PUNCT
eurjchem-1701	131	29	.	.	PUNCT
eurjchem-1701	132	1	1h	1h	NUM
eurjchem-1701	132	2	nmr	nmr	NOUN
eurjchem-1701	132	3	(	(	PUNCT
eurjchem-1701	132	4	300	300	NUM
eurjchem-1701	132	5	mhz	mhz	NOUN
eurjchem-1701	132	6	,	,	PUNCT
eurjchem-1701	132	7	dmso	dmso	NOUN
eurjchem-1701	132	8	-	-	NOUN
eurjchem-1701	132	9	d6	d6	NOUN
eurjchem-1701	132	10	,	,	PUNCT
eurjchem-1701	132	11	δ	δ	PROPN
eurjchem-1701	132	12	,	,	PUNCT
eurjchem-1701	132	13	ppm	ppm	NUM
eurjchem-1701	132	14	):	):	PUNCT
eurjchem-1701	132	15	8.06	8.06	NUM
eurjchem-1701	132	16	-	-	SYM
eurjchem-1701	132	17	7.18	7.18	NUM
eurjchem-1701	132	18	(	(	PUNCT
eurjchem-1701	132	19	m	m	PROPN
eurjchem-1701	132	20	,	,	PUNCT
eurjchem-1701	132	21	8h	8h	NUM
eurjchem-1701	132	22	,	,	PUNCT
eurjchem-1701	132	23	arh	arh	PROPN
eurjchem-1701	132	24	’s	’s	PART
eurjchem-1701	132	25	+	+	NUM
eurjchem-1701	132	26	thiophene	thiophene	NOUN
eurjchem-1701	132	27	protons	proton	NOUN
eurjchem-1701	132	28	)	)	PUNCT
eurjchem-1701	132	29	,	,	PUNCT
eurjchem-1701	132	30	10.41	10.41	NUM
eurjchem-1701	132	31	(	(	PUNCT
eurjchem-1701	132	32	s	s	PROPN
eurjchem-1701	132	33	,	,	PUNCT
eurjchem-1701	132	34	1h	1h	NUM
eurjchem-1701	132	35	,	,	PUNCT
eurjchem-1701	132	36	nh	nh	PROPN
eurjchem-1701	132	37	)	)	PUNCT
eurjchem-1701	132	38	.	.	PUNCT
eurjchem-1701	133	1	13c	13c	NOUN
eurjchem-1701	133	2	nmr	nmr	NOUN
eurjchem-1701	133	3	(	(	PUNCT
eurjchem-1701	133	4	75.4	75.4	NUM
eurjchem-1701	133	5	mhz	mhz	NOUN
eurjchem-1701	133	6	,	,	PUNCT
eurjchem-1701	133	7	dmso	dmso	NOUN
eurjchem-1701	133	8	-	-	NOUN
eurjchem-1701	133	9	d6	d6	NOUN
eurjchem-1701	133	10	,	,	PUNCT
eurjchem-1701	133	11	δ	δ	PROPN
eurjchem-1701	133	12	,	,	PUNCT
eurjchem-1701	133	13	ppm	ppm	NUM
eurjchem-1701	133	14	):	):	PUNCT
eurjchem-1701	133	15	167.1	167.1	NUM
eurjchem-1701	133	16	(	(	PUNCT
eurjchem-1701	133	17	1c	1c	NOUN
eurjchem-1701	133	18	,	,	PUNCT
eurjchem-1701	133	19	ncs	ncs	NOUN
eurjchem-1701	133	20	)	)	PUNCT
eurjchem-1701	133	21	,	,	PUNCT
eurjchem-1701	133	22	156.1	156.1	NUM
eurjchem-1701	133	23	(	(	PUNCT
eurjchem-1701	133	24	1c	1c	X
eurjchem-1701	133	25	,	,	PUNCT
eurjchem-1701	133	26	ncn	ncn	NOUN
eurjchem-1701	133	27	)	)	PUNCT
eurjchem-1701	133	28	,	,	PUNCT
eurjchem-1701	133	29	135.8	135.8	NUM
eurjchem-1701	133	30	,	,	PUNCT
eurjchem-1701	133	31	129.7	129.7	NUM
eurjchem-1701	133	32	,	,	PUNCT
eurjchem-1701	133	33	129.1	129.1	NUM
eurjchem-1701	133	34	,	,	PUNCT
eurjchem-1701	133	35	128.4	128.4	NUM
eurjchem-1701	133	36	,	,	PUNCT
eurjchem-1701	133	37	128.3	128.3	NUM
eurjchem-1701	133	38	,	,	PUNCT
eurjchem-1701	133	39	127.1	127.1	NUM
eurjchem-1701	133	40	,	,	PUNCT
eurjchem-1701	133	41	121.4	121.4	NUM
eurjchem-1701	133	42	,	,	PUNCT
eurjchem-1701	133	43	120.2	120.2	NUM
eurjchem-1701	133	44	(	(	PUNCT
eurjchem-1701	133	45	ar	ar	NOUN
eurjchem-1701	133	46	-	-	NOUN
eurjchem-1701	133	47	c	c	NOUN
eurjchem-1701	133	48	)	)	PUNCT
eurjchem-1701	133	49	.	.	PUNCT
eurjchem-1701	134	1	ms	ms	NOUN
eurjchem-1701	134	2	(	(	PUNCT
eurjchem-1701	134	3	ei	ei	PROPN
eurjchem-1701	134	4	,	,	PUNCT
eurjchem-1701	134	5	m	m	PROPN
eurjchem-1701	134	6	/	/	SYM
eurjchem-1701	134	7	z	z	PROPN
eurjchem-1701	134	8	(	(	PUNCT
eurjchem-1701	134	9	%	%	NOUN
eurjchem-1701	134	10	)	)	PUNCT
eurjchem-1701	134	11	):	):	PUNCT
eurjchem-1701	134	12	259	259	NUM
eurjchem-1701	134	13	(	(	PUNCT
eurjchem-1701	134	14	m+	m+	NUM
eurjchem-1701	134	15	,	,	PUNCT
eurjchem-1701	134	16	100	100	NUM
eurjchem-1701	134	17	)	)	PUNCT
eurjchem-1701	134	18	,	,	PUNCT
eurjchem-1701	134	19	200	200	NUM
eurjchem-1701	134	20	(	(	PUNCT
eurjchem-1701	134	21	10	10	NUM
eurjchem-1701	134	22	)	)	PUNCT
eurjchem-1701	134	23	,	,	PUNCT
eurjchem-1701	134	24	149	149	NUM
eurjchem-1701	134	25	(	(	PUNCT
eurjchem-1701	134	26	5	5	NUM
eurjchem-1701	134	27	)	)	PUNCT
eurjchem-1701	134	28	,	,	PUNCT
eurjchem-1701	134	29	108	108	NUM
eurjchem-1701	134	30	(	(	PUNCT
eurjchem-1701	134	31	10	10	NUM
eurjchem-1701	134	32	)	)	PUNCT
eurjchem-1701	134	33	,	,	PUNCT
eurjchem-1701	134	34	91	91	NUM
eurjchem-1701	134	35	(	(	PUNCT
eurjchem-1701	134	36	25	25	NUM
eurjchem-1701	134	37	)	)	PUNCT
eurjchem-1701	134	38	.	.	PUNCT
eurjchem-1701	135	1	anal	anal	PROPN
eurjchem-1701	135	2	.	.	PUNCT
eurjchem-1701	135	3	calcd	calcd	NOUN
eurjchem-1701	135	4	.	.	PUNCT
eurjchem-1701	136	1	for	for	SCONJ
eurjchem-1701	136	2	c12h9n3s2	c12h9n3s2	NOUN
eurjchem-1701	136	3	:	:	PUNCT
eurjchem-1701	136	4	c	c	X
eurjchem-1701	136	5	,	,	PUNCT
eurjchem-1701	136	6	55.57	55.57	NUM
eurjchem-1701	136	7	;	;	PUNCT
eurjchem-1701	136	8	h	h	NOUN
eurjchem-1701	136	9	,	,	PUNCT
eurjchem-1701	136	10	3.50	3.50	NUM
eurjchem-1701	136	11	;	;	PUNCT
eurjchem-1701	136	12	n	n	CCONJ
eurjchem-1701	136	13	,	,	PUNCT
eurjchem-1701	136	14	16.20	16.20	NUM
eurjchem-1701	136	15	.	.	PUNCT
eurjchem-1701	136	16	found	find	VERB
eurjchem-1701	136	17	:	:	PUNCT
eurjchem-1701	137	1	c	c	X
eurjchem-1701	137	2	,	,	PUNCT
eurjchem-1701	137	3	55.46	55.46	NUM
eurjchem-1701	137	4	;	;	PUNCT
eurjchem-1701	137	5	h	h	NOUN
eurjchem-1701	137	6	,	,	PUNCT
eurjchem-1701	137	7	3.39	3.39	NUM
eurjchem-1701	137	8	;	;	PUNCT
eurjchem-1701	137	9	n	n	CCONJ
eurjchem-1701	137	10	,	,	PUNCT
eurjchem-1701	137	11	16.10	16.10	NUM
eurjchem-1701	137	12	%	%	NOUN
eurjchem-1701	137	13	.	.	PUNCT
eurjchem-1701	138	1	2.3.8	2.3.8	NUM
eurjchem-1701	138	2	.	.	PUNCT
eurjchem-1701	139	1	synthesis	synthesis	NOUN
eurjchem-1701	139	2	of	of	ADP
eurjchem-1701	139	3	n-(2	n-(2	NOUN
eurjchem-1701	139	4	-	-	PUNCT
eurjchem-1701	139	5	isonicotinoylhydrazinecarbonothioyl)thiophene-2	isonicotinoylhydrazinecarbonothioyl)thiophene-2	NOUN
eurjchem-1701	139	6	-	-	PUNCT
eurjchem-1701	139	7	carboxamide	carboxamide	NOUN
eurjchem-1701	139	8	(	(	PUNCT
eurjchem-1701	139	9	11	11	NUM
eurjchem-1701	139	10	)	)	PUNCT
eurjchem-1701	139	11	a	a	DET
eurjchem-1701	139	12	mixture	mixture	NOUN
eurjchem-1701	139	13	of	of	ADP
eurjchem-1701	139	14	thiophene-2	thiophene-2	NOUN
eurjchem-1701	139	15	-	-	PUNCT
eurjchem-1701	139	16	carbonylisothiocyanate	carbonylisothiocyanate	NOUN
eurjchem-1701	139	17	(	(	PUNCT
eurjchem-1701	139	18	1	1	NUM
eurjchem-1701	139	19	)	)	PUNCT
eurjchem-1701	139	20	(	(	PUNCT
eurjchem-1701	139	21	10.0	10.0	NUM
eurjchem-1701	139	22	mol	mol	NOUN
eurjchem-1701	139	23	)	)	PUNCT
eurjchem-1701	139	24	isonicotinohydrazide	isonicotinohydrazide	NOUN
eurjchem-1701	139	25	(	(	PUNCT
eurjchem-1701	139	26	10.0	10.0	NUM
eurjchem-1701	139	27	mol	mol	NOUN
eurjchem-1701	139	28	)	)	PUNCT
eurjchem-1701	139	29	in	in	ADP
eurjchem-1701	139	30	dioxane	dioxane	NOUN
eurjchem-1701	139	31	(	(	PUNCT
eurjchem-1701	139	32	50	50	NUM
eurjchem-1701	139	33	ml	ml	NOUN
eurjchem-1701	139	34	)	)	PUNCT
eurjchem-1701	139	35	was	be	AUX
eurjchem-1701	139	36	stirred	stir	VERB
eurjchem-1701	139	37	at	at	ADP
eurjchem-1701	139	38	room	room	NOUN
eurjchem-1701	139	39	temperature	temperature	NOUN
eurjchem-1701	139	40	for	for	ADP
eurjchem-1701	139	41	1	1	NUM
eurjchem-1701	139	42	h.	h.	NOUN
eurjchem-1701	139	43	the	the	DET
eurjchem-1701	139	44	reaction	reaction	NOUN
eurjchem-1701	139	45	mixture	mixture	NOUN
eurjchem-1701	139	46	was	be	AUX
eurjchem-1701	139	47	poured	pour	VERB
eurjchem-1701	139	48	into	into	ADP
eurjchem-1701	139	49	water	water	NOUN
eurjchem-1701	139	50	.	.	PUNCT
eurjchem-1701	140	1	the	the	DET
eurjchem-1701	140	2	formed	form	VERB
eurjchem-1701	140	3	precipitate	precipitate	NOUN
eurjchem-1701	140	4	was	be	AUX
eurjchem-1701	140	5	filtered	filter	VERB
eurjchem-1701	140	6	off	off	ADP
eurjchem-1701	140	7	,	,	PUNCT
eurjchem-1701	140	8	washed	wash	VERB
eurjchem-1701	140	9	with	with	ADP
eurjchem-1701	140	10	water	water	NOUN
eurjchem-1701	140	11	,	,	PUNCT
eurjchem-1701	140	12	dried	dry	VERB
eurjchem-1701	140	13	and	and	CCONJ
eurjchem-1701	140	14	crystallized	crystallize	VERB
eurjchem-1701	140	15	from	from	ADP
eurjchem-1701	140	16	ethanol	ethanol	NOUN
eurjchem-1701	140	17	to	to	PART
eurjchem-1701	140	18	give	give	VERB
eurjchem-1701	140	19	compound	compound	NOUN
eurjchem-1701	140	20	11	11	NUM
eurjchem-1701	140	21	(	(	PUNCT
eurjchem-1701	140	22	scheme	scheme	NOUN
eurjchem-1701	140	23	4	4	NUM
eurjchem-1701	140	24	)	)	PUNCT
eurjchem-1701	140	25	.	.	PUNCT
eurjchem-1701	141	1	color	color	NOUN
eurjchem-1701	141	2	:	:	PUNCT
eurjchem-1701	141	3	yellow	yellow	ADJ
eurjchem-1701	141	4	.	.	PUNCT
eurjchem-1701	142	1	yield	yield	NOUN
eurjchem-1701	142	2	:	:	PUNCT
eurjchem-1701	142	3	58	58	NUM
eurjchem-1701	142	4	%	%	NOUN
eurjchem-1701	142	5	.	.	PUNCT
eurjchem-1701	143	1	m.p	m.p	PROPN
eurjchem-1701	143	2	.	.	PROPN
eurjchem-1701	143	3	:	:	PUNCT
eurjchem-1701	144	1	212	212	NUM
eurjchem-1701	144	2	-	-	SYM
eurjchem-1701	144	3	213	213	NUM
eurjchem-1701	144	4	°	°	NOUN
eurjchem-1701	144	5	c	c	NOUN
eurjchem-1701	144	6	.	.	PUNCT
eurjchem-1701	145	1	ft	ft	PROPN
eurjchem-1701	145	2	-	-	PUNCT
eurjchem-1701	145	3	ir	ir	PROPN
eurjchem-1701	145	4	(	(	PUNCT
eurjchem-1701	145	5	kbr	kbr	PROPN
eurjchem-1701	145	6	,	,	PUNCT
eurjchem-1701	145	7	ν	ν	PROPN
eurjchem-1701	145	8	,	,	PUNCT
eurjchem-1701	145	9	cm-1	cm-1	NUM
eurjchem-1701	145	10	):	):	PUNCT
eurjchem-1701	145	11	3419	3419	NUM
eurjchem-1701	145	12	,	,	PUNCT
eurjchem-1701	145	13	3252	3252	NUM
eurjchem-1701	145	14	(	(	PUNCT
eurjchem-1701	145	15	nh	nh	NOUN
eurjchem-1701	145	16	)	)	PUNCT
eurjchem-1701	145	17	,	,	PUNCT
eurjchem-1701	145	18	3018	3018	NUM
eurjchem-1701	145	19	(	(	PUNCT
eurjchem-1701	145	20	ch	ch	NOUN
eurjchem-1701	145	21	arom	arom	NOUN
eurjchem-1701	145	22	.	.	PUNCT
eurjchem-1701	145	23	)	)	PUNCT
eurjchem-1701	145	24	,	,	PUNCT
eurjchem-1701	145	25	1671	1671	NUM
eurjchem-1701	145	26	,	,	PUNCT
eurjchem-1701	145	27	1666	1666	NUM
eurjchem-1701	145	28	(	(	PUNCT
eurjchem-1701	145	29	2c	2c	NOUN
eurjchem-1701	145	30	=	=	SYM
eurjchem-1701	145	31	o	o	NOUN
eurjchem-1701	145	32	)	)	PUNCT
eurjchem-1701	145	33	.	.	PUNCT
eurjchem-1701	146	1	1h	1h	NUM
eurjchem-1701	146	2	nmr	nmr	NOUN
eurjchem-1701	146	3	(	(	PUNCT
eurjchem-1701	146	4	300	300	NUM
eurjchem-1701	146	5	mhz	mhz	NOUN
eurjchem-1701	146	6	,	,	PUNCT
eurjchem-1701	146	7	dmso	dmso	NOUN
eurjchem-1701	146	8	-	-	NOUN
eurjchem-1701	146	9	d6	d6	NOUN
eurjchem-1701	146	10	,	,	PUNCT
eurjchem-1701	146	11	δ	δ	PROPN
eurjchem-1701	146	12	,	,	PUNCT
eurjchem-1701	146	13	ppm	ppm	NOUN
eurjchem-1701	146	14	):	):	PUNCT
eurjchem-1701	146	15	7.98	7.98	NUM
eurjchem-1701	146	16	-	-	SYM
eurjchem-1701	146	17	7.24	7.24	NUM
eurjchem-1701	146	18	(	(	PUNCT
eurjchem-1701	146	19	m	m	PROPN
eurjchem-1701	146	20	,	,	PUNCT
eurjchem-1701	146	21	7h	7h	PROPN
eurjchem-1701	146	22	,	,	PUNCT
eurjchem-1701	146	23	arh	arh	PROPN
eurjchem-1701	146	24	’s	’s	PART
eurjchem-1701	146	25	+	+	NUM
eurjchem-1701	146	26	thiophene	thiophene	NOUN
eurjchem-1701	146	27	protons	proton	NOUN
eurjchem-1701	146	28	)	)	PUNCT
eurjchem-1701	146	29	,	,	PUNCT
eurjchem-1701	146	30	11.41	11.41	NUM
eurjchem-1701	146	31	(	(	PUNCT
eurjchem-1701	146	32	s	s	PROPN
eurjchem-1701	146	33	,	,	PUNCT
eurjchem-1701	146	34	1h	1h	NUM
eurjchem-1701	146	35	,	,	PUNCT
eurjchem-1701	146	36	d2o	d2o	NOUN
eurjchem-1701	146	37	exchangeable	exchangeable	ADJ
eurjchem-1701	146	38	,	,	PUNCT
eurjchem-1701	146	39	nh	nh	PROPN
eurjchem-1701	146	40	)	)	PUNCT
eurjchem-1701	146	41	,	,	PUNCT
eurjchem-1701	146	42	11.85	11.85	NUM
eurjchem-1701	146	43	(	(	PUNCT
eurjchem-1701	146	44	s	s	PROPN
eurjchem-1701	146	45	,	,	PUNCT
eurjchem-1701	146	46	1h	1h	NUM
eurjchem-1701	146	47	,	,	PUNCT
eurjchem-1701	146	48	d2o	d2o	NOUN
eurjchem-1701	146	49	exchangeable	exchangeable	ADJ
eurjchem-1701	146	50	,	,	PUNCT
eurjchem-1701	146	51	nh	nh	PROPN
eurjchem-1701	146	52	)	)	PUNCT
eurjchem-1701	146	53	,	,	PUNCT
eurjchem-1701	146	54	12.15	12.15	NUM
eurjchem-1701	146	55	(	(	PUNCT
eurjchem-1701	146	56	s	s	PROPN
eurjchem-1701	146	57	,	,	PUNCT
eurjchem-1701	146	58	1h	1h	NUM
eurjchem-1701	146	59	,	,	PUNCT
eurjchem-1701	146	60	d2o	d2o	NOUN
eurjchem-1701	146	61	exchangeable	exchangeable	ADJ
eurjchem-1701	146	62	,	,	PUNCT
eurjchem-1701	146	63	nh	nh	PROPN
eurjchem-1701	146	64	)	)	PUNCT
eurjchem-1701	146	65	.	.	PUNCT
eurjchem-1701	147	1	13c	13c	NOUN
eurjchem-1701	147	2	nmr	nmr	NOUN
eurjchem-1701	147	3	(	(	PUNCT
eurjchem-1701	147	4	75.4	75.4	NUM
eurjchem-1701	147	5	mhz	mhz	NOUN
eurjchem-1701	147	6	,	,	PUNCT
eurjchem-1701	147	7	dmso	dmso	NOUN
eurjchem-1701	147	8	-	-	NOUN
eurjchem-1701	147	9	d6	d6	NOUN
eurjchem-1701	147	10	,	,	PUNCT
eurjchem-1701	147	11	δ	δ	PROPN
eurjchem-1701	147	12	,	,	PUNCT
eurjchem-1701	147	13	ppm	ppm	NUM
eurjchem-1701	147	14	):	):	PUNCT
eurjchem-1701	147	15	167.1	167.1	NUM
eurjchem-1701	147	16	(	(	PUNCT
eurjchem-1701	147	17	1c	1c	NOUN
eurjchem-1701	147	18	,	,	PUNCT
eurjchem-1701	147	19	ncs	ncs	NOUN
eurjchem-1701	147	20	)	)	PUNCT
eurjchem-1701	147	21	,	,	PUNCT
eurjchem-1701	147	22	156.1	156.1	NUM
eurjchem-1701	147	23	(	(	PUNCT
eurjchem-1701	147	24	1c	1c	X
eurjchem-1701	147	25	,	,	PUNCT
eurjchem-1701	147	26	ncn	ncn	NOUN
eurjchem-1701	147	27	)	)	PUNCT
eurjchem-1701	147	28	,	,	PUNCT
eurjchem-1701	147	29	135.8	135.8	NUM
eurjchem-1701	147	30	,	,	PUNCT
eurjchem-1701	147	31	129.7	129.7	NUM
eurjchem-1701	147	32	,	,	PUNCT
eurjchem-1701	147	33	129.1	129.1	NUM
eurjchem-1701	147	34	,	,	PUNCT
eurjchem-1701	147	35	128.4	128.4	NUM
eurjchem-1701	147	36	,	,	PUNCT
eurjchem-1701	147	37	128.3	128.3	NUM
eurjchem-1701	147	38	,	,	PUNCT
eurjchem-1701	147	39	127.1	127.1	NUM
eurjchem-1701	147	40	,	,	PUNCT
eurjchem-1701	147	41	121.4	121.4	NUM
eurjchem-1701	147	42	,	,	PUNCT
eurjchem-1701	147	43	120.2	120.2	NUM
eurjchem-1701	147	44	(	(	PUNCT
eurjchem-1701	147	45	ar	ar	NOUN
eurjchem-1701	147	46	-	-	NOUN
eurjchem-1701	147	47	c	c	NOUN
eurjchem-1701	147	48	)	)	PUNCT
eurjchem-1701	147	49	.	.	PUNCT
eurjchem-1701	148	1	ms	ms	NOUN
eurjchem-1701	148	2	(	(	PUNCT
eurjchem-1701	148	3	ei	ei	PROPN
eurjchem-1701	148	4	,	,	PUNCT
eurjchem-1701	148	5	m	m	PROPN
eurjchem-1701	148	6	/	/	SYM
eurjchem-1701	148	7	z	z	PROPN
eurjchem-1701	148	8	(	(	PUNCT
eurjchem-1701	148	9	%	%	NOUN
eurjchem-1701	148	10	)	)	PUNCT
eurjchem-1701	148	11	):	):	PUNCT
eurjchem-1701	148	12	306	306	NUM
eurjchem-1701	148	13	(	(	PUNCT
eurjchem-1701	148	14	m+	m+	NUM
eurjchem-1701	148	15	,	,	PUNCT
eurjchem-1701	148	16	100	100	NUM
eurjchem-1701	148	17	)	)	PUNCT
eurjchem-1701	148	18	,	,	PUNCT
eurjchem-1701	148	19	273	273	NUM
eurjchem-1701	148	20	(	(	PUNCT
eurjchem-1701	148	21	15	15	NUM
eurjchem-1701	148	22	)	)	PUNCT
eurjchem-1701	148	23	,	,	PUNCT
eurjchem-1701	148	24	170	170	NUM
eurjchem-1701	148	25	(	(	PUNCT
eurjchem-1701	148	26	5	5	NUM
eurjchem-1701	148	27	)	)	PUNCT
eurjchem-1701	148	28	,	,	PUNCT
eurjchem-1701	148	29	137	137	NUM
eurjchem-1701	148	30	(	(	PUNCT
eurjchem-1701	148	31	5	5	NUM
eurjchem-1701	148	32	)	)	PUNCT
eurjchem-1701	148	33	,	,	PUNCT
eurjchem-1701	148	34	110	110	NUM
eurjchem-1701	148	35	(	(	PUNCT
eurjchem-1701	148	36	10	10	NUM
eurjchem-1701	148	37	)	)	PUNCT
eurjchem-1701	148	38	,	,	PUNCT
eurjchem-1701	148	39	78	78	NUM
eurjchem-1701	148	40	(	(	PUNCT
eurjchem-1701	148	41	30	30	NUM
eurjchem-1701	148	42	)	)	PUNCT
eurjchem-1701	148	43	.	.	PUNCT
eurjchem-1701	149	1	2.3.9	2.3.9	X
eurjchem-1701	149	2	.	.	PUNCT
eurjchem-1701	150	1	synthesis	synthesis	NOUN
eurjchem-1701	150	2	of	of	ADP
eurjchem-1701	150	3	n-(5-(pyridin-4	n-(5-(pyridin-4	NOUN
eurjchem-1701	150	4	-	-	PUNCT
eurjchem-1701	150	5	yl)-1,3,4	yl)-1,3,4	NOUN
eurjchem-1701	150	6	-	-	PUNCT
eurjchem-1701	150	7	thiadiazol-2yl)thiophene-2	thiadiazol-2yl)thiophene-2	NOUN
eurjchem-1701	150	8	-	-	PUNCT
eurjchem-1701	150	9	carboxamide	carboxamide	NOUN
eurjchem-1701	150	10	(	(	PUNCT
eurjchem-1701	150	11	12	12	NUM
eurjchem-1701	150	12	)	)	PUNCT
eurjchem-1701	150	13	a	a	DET
eurjchem-1701	150	14	mixture	mixture	NOUN
eurjchem-1701	150	15	of	of	ADP
eurjchem-1701	150	16	n-(2	n-(2	PROPN
eurjchem-1701	150	17	-	-	PUNCT
eurjchem-1701	150	18	isonicotinoylhydrazinecarbonothioyl	isonicotinoylhydrazinecarbonothioyl	ADJ
eurjchem-1701	150	19	)	)	PUNCT
eurjchem-1701	150	20	thiophene-2	thiophene-2	NUM
eurjchem-1701	150	21	-	-	PUNCT
eurjchem-1701	150	22	carboxamide	carboxamide	NOUN
eurjchem-1701	150	23	(	(	PUNCT
eurjchem-1701	150	24	11	11	NUM
eurjchem-1701	150	25	)	)	PUNCT
eurjchem-1701	150	26	(	(	PUNCT
eurjchem-1701	150	27	1.20	1.20	NUM
eurjchem-1701	150	28	mol	mol	NOUN
eurjchem-1701	150	29	)	)	PUNCT
eurjchem-1701	150	30	and	and	CCONJ
eurjchem-1701	150	31	sulfuric	sulfuric	ADJ
eurjchem-1701	150	32	acid	acid	NOUN
eurjchem-1701	150	33	(	(	PUNCT
eurjchem-1701	150	34	1.20	1.20	NUM
eurjchem-1701	150	35	mol	mol	NOUN
eurjchem-1701	150	36	)	)	PUNCT
eurjchem-1701	150	37	in	in	ADP
eurjchem-1701	150	38	ethanol	ethanol	NOUN
eurjchem-1701	150	39	(	(	PUNCT
eurjchem-1701	150	40	20	20	NUM
eurjchem-1701	150	41	ml	ml	NOUN
eurjchem-1701	150	42	)	)	PUNCT
eurjchem-1701	150	43	was	be	AUX
eurjchem-1701	150	44	heated	heat	VERB
eurjchem-1701	150	45	under	under	ADP
eurjchem-1701	150	46	reflux	reflux	NOUN
eurjchem-1701	150	47	for	for	ADP
eurjchem-1701	150	48	6	6	NUM
eurjchem-1701	150	49	h.	h.	NOUN
eurjchem-1701	150	50	the	the	DET
eurjchem-1701	150	51	reaction	reaction	NOUN
eurjchem-1701	150	52	mixture	mixture	NOUN
eurjchem-1701	150	53	was	be	AUX
eurjchem-1701	150	54	poured	pour	VERB
eurjchem-1701	150	55	into	into	ADP
eurjchem-1701	150	56	water	water	NOUN
eurjchem-1701	150	57	.	.	PUNCT
eurjchem-1701	151	1	the	the	DET
eurjchem-1701	151	2	formed	form	VERB
eurjchem-1701	151	3	precipitate	precipitate	NOUN
eurjchem-1701	151	4	was	be	AUX
eurjchem-1701	151	5	filtered	filter	VERB
eurjchem-1701	151	6	off	off	ADP
eurjchem-1701	151	7	,	,	PUNCT
eurjchem-1701	151	8	dried	dry	VERB
eurjchem-1701	151	9	and	and	CCONJ
eurjchem-1701	151	10	crystallized	crystallize	VERB
eurjchem-1701	151	11	from	from	ADP
eurjchem-1701	151	12	ethanol	ethanol	NOUN
eurjchem-1701	151	13	to	to	PART
eurjchem-1701	151	14	give	give	VERB
eurjchem-1701	151	15	compound	compound	NOUN
eurjchem-1701	151	16	12	12	NUM
eurjchem-1701	151	17	(	(	PUNCT
eurjchem-1701	151	18	scheme	scheme	NOUN
eurjchem-1701	151	19	4	4	NUM
eurjchem-1701	151	20	)	)	PUNCT
eurjchem-1701	151	21	.	.	PUNCT
eurjchem-1701	152	1	color	color	NOUN
eurjchem-1701	152	2	:	:	PUNCT
eurjchem-1701	152	3	white	white	ADJ
eurjchem-1701	152	4	.	.	PUNCT
eurjchem-1701	153	1	yield	yield	NOUN
eurjchem-1701	153	2	:	:	PUNCT
eurjchem-1701	153	3	95	95	NUM
eurjchem-1701	153	4	%	%	NOUN
eurjchem-1701	153	5	.	.	PUNCT
eurjchem-1701	154	1	m.p	m.p	PROPN
eurjchem-1701	154	2	.	.	PROPN
eurjchem-1701	154	3	:	:	PUNCT
eurjchem-1701	155	1	320	320	NUM
eurjchem-1701	155	2	-	-	SYM
eurjchem-1701	155	3	321	321	NUM
eurjchem-1701	155	4	°	°	NUM
eurjchem-1701	155	5	c	c	NOUN
eurjchem-1701	155	6	.	.	PUNCT
eurjchem-1701	155	7	ft	ft	PROPN
eurjchem-1701	155	8	-	-	PUNCT
eurjchem-1701	155	9	ir	ir	PROPN
eurjchem-1701	155	10	(	(	PUNCT
eurjchem-1701	155	11	kbr	kbr	PROPN
eurjchem-1701	155	12	,	,	PUNCT
eurjchem-1701	155	13	ν	ν	PROPN
eurjchem-1701	155	14	,	,	PUNCT
eurjchem-1701	155	15	cm-1	cm-1	NUM
eurjchem-1701	155	16	):	):	PUNCT
eurjchem-1701	155	17	3386	3386	NUM
eurjchem-1701	155	18	(	(	PUNCT
eurjchem-1701	155	19	nh	nh	NOUN
eurjchem-1701	155	20	)	)	PUNCT
eurjchem-1701	155	21	,	,	PUNCT
eurjchem-1701	155	22	1662	1662	NUM
eurjchem-1701	155	23	(	(	PUNCT
eurjchem-1701	155	24	c	c	NOUN
eurjchem-1701	155	25	=	=	NOUN
eurjchem-1701	155	26	o	o	NOUN
eurjchem-1701	155	27	)	)	PUNCT
eurjchem-1701	155	28	(	(	PUNCT
eurjchem-1701	155	29	amide	amide	NOUN
eurjchem-1701	155	30	)	)	PUNCT
eurjchem-1701	155	31	,	,	PUNCT
eurjchem-1701	155	32	1637	1637	NUM
eurjchem-1701	155	33	(	(	PUNCT
eurjchem-1701	155	34	c	c	NOUN
eurjchem-1701	155	35	=	=	SYM
eurjchem-1701	155	36	n	n	NUM
eurjchem-1701	155	37	)	)	PUNCT
eurjchem-1701	155	38	,	,	PUNCT
eurjchem-1701	155	39	1628	1628	NUM
eurjchem-1701	155	40	(	(	PUNCT
eurjchem-1701	155	41	c	c	NOUN
eurjchem-1701	155	42	=	=	SYM
eurjchem-1701	155	43	c	c	NOUN
eurjchem-1701	155	44	)	)	PUNCT
eurjchem-1701	155	45	.	.	PUNCT
eurjchem-1701	156	1	1h	1h	NUM
eurjchem-1701	156	2	nmr	nmr	NOUN
eurjchem-1701	156	3	(	(	PUNCT
eurjchem-1701	156	4	300	300	NUM
eurjchem-1701	156	5	mhz	mhz	NOUN
eurjchem-1701	156	6	,	,	PUNCT
eurjchem-1701	156	7	dmsod6	dmsod6	PROPN
eurjchem-1701	156	8	,	,	PUNCT
eurjchem-1701	156	9	δ	δ	PROPN
eurjchem-1701	156	10	,	,	PUNCT
eurjchem-1701	156	11	ppm	ppm	NUM
eurjchem-1701	156	12	):	):	PUNCT
eurjchem-1701	156	13	8.97	8.97	NUM
eurjchem-1701	156	14	-	-	SYM
eurjchem-1701	156	15	7.30	7.30	NUM
eurjchem-1701	156	16	(	(	PUNCT
eurjchem-1701	156	17	m	m	PROPN
eurjchem-1701	156	18	,	,	PUNCT
eurjchem-1701	156	19	7h	7h	PROPN
eurjchem-1701	156	20	,	,	PUNCT
eurjchem-1701	156	21	arh	arh	PROPN
eurjchem-1701	156	22	’s	’s	PART
eurjchem-1701	156	23	+	+	NUM
eurjchem-1701	156	24	thiophene	thiophene	NOUN
eurjchem-1701	156	25	protons	proton	NOUN
eurjchem-1701	156	26	)	)	PUNCT
eurjchem-1701	156	27	,	,	PUNCT
eurjchem-1701	156	28	8.98	8.98	NUM
eurjchem-1701	156	29	(	(	PUNCT
eurjchem-1701	156	30	s	s	PROPN
eurjchem-1701	156	31	,	,	PUNCT
eurjchem-1701	156	32	1h	1h	NUM
eurjchem-1701	156	33	,	,	PUNCT
eurjchem-1701	156	34	d2o	d2o	NOUN
eurjchem-1701	156	35	exchangeable	exchangeable	ADJ
eurjchem-1701	156	36	,	,	PUNCT
eurjchem-1701	156	37	nh	nh	PROPN
eurjchem-1701	156	38	)	)	PUNCT
eurjchem-1701	156	39	.	.	PUNCT
eurjchem-1701	157	1	13c	13c	NOUN
eurjchem-1701	157	2	nmr	nmr	NOUN
eurjchem-1701	157	3	(	(	PUNCT
eurjchem-1701	157	4	75.4	75.4	NUM
eurjchem-1701	157	5	mhz	mhz	NOUN
eurjchem-1701	157	6	,	,	PUNCT
eurjchem-1701	157	7	dmso	dmso	NOUN
eurjchem-1701	157	8	-	-	NOUN
eurjchem-1701	157	9	d6	d6	NOUN
eurjchem-1701	157	10	,	,	PUNCT
eurjchem-1701	157	11	δ	δ	PROPN
eurjchem-1701	157	12	,	,	PUNCT
eurjchem-1701	157	13	ppm	ppm	NUM
eurjchem-1701	157	14	):	):	PUNCT
eurjchem-1701	157	15	162.4	162.4	NUM
eurjchem-1701	157	16	(	(	PUNCT
eurjchem-1701	157	17	1c	1c	NOUN
eurjchem-1701	157	18	,	,	PUNCT
eurjchem-1701	157	19	c	c	NOUN
eurjchem-1701	157	20	=	=	SYM
eurjchem-1701	157	21	o	o	NOUN
eurjchem-1701	157	22	)	)	PUNCT
eurjchem-1701	157	23	,	,	PUNCT
eurjchem-1701	157	24	156.4	156.4	NUM
eurjchem-1701	157	25	,	,	PUNCT
eurjchem-1701	157	26	152.1	152.1	NUM
eurjchem-1701	157	27	(	(	PUNCT
eurjchem-1701	157	28	2c	2c	NUM
eurjchem-1701	157	29	,	,	PUNCT
eurjchem-1701	157	30	triazole	triazole	NOUN
eurjchem-1701	157	31	ring	ring	NOUN
eurjchem-1701	157	32	)	)	PUNCT
eurjchem-1701	157	33	,	,	PUNCT
eurjchem-1701	157	34	149.0	149.0	NUM
eurjchem-1701	157	35	,	,	PUNCT
eurjchem-1701	157	36	135.3	135.3	NUM
eurjchem-1701	157	37	,	,	PUNCT
eurjchem-1701	157	38	121.4	121.4	NUM
eurjchem-1701	157	39	,	,	PUNCT
eurjchem-1701	157	40	137.8	137.8	NUM
eurjchem-1701	157	41	,	,	PUNCT
eurjchem-1701	157	42	129.2	129.2	NUM
eurjchem-1701	157	43	,	,	PUNCT
eurjchem-1701	157	44	128.4	128.4	NUM
eurjchem-1701	157	45	,	,	PUNCT
eurjchem-1701	157	46	127.0	127.0	NUM
eurjchem-1701	157	47	(	(	PUNCT
eurjchem-1701	157	48	ar	ar	NOUN
eurjchem-1701	157	49	-	-	NOUN
eurjchem-1701	157	50	c	c	NOUN
eurjchem-1701	157	51	)	)	PUNCT
eurjchem-1701	157	52	.	.	PUNCT
eurjchem-1701	158	1	ms	ms	NOUN
eurjchem-1701	158	2	(	(	PUNCT
eurjchem-1701	158	3	ei	ei	PROPN
eurjchem-1701	158	4	,	,	PUNCT
eurjchem-1701	158	5	m	m	PROPN
eurjchem-1701	158	6	/	/	SYM
eurjchem-1701	158	7	z	z	PROPN
eurjchem-1701	158	8	(	(	PUNCT
eurjchem-1701	158	9	%	%	NOUN
eurjchem-1701	158	10	)	)	PUNCT
eurjchem-1701	158	11	):	):	PUNCT
eurjchem-1701	158	12	288	288	NUM
eurjchem-1701	158	13	(	(	PUNCT
eurjchem-1701	158	14	m+	m+	NUM
eurjchem-1701	158	15	,	,	PUNCT
eurjchem-1701	158	16	60	60	NUM
eurjchem-1701	158	17	)	)	PUNCT
eurjchem-1701	158	18	,	,	PUNCT
eurjchem-1701	158	19	261	261	NUM
eurjchem-1701	158	20	(	(	PUNCT
eurjchem-1701	158	21	100	100	NUM
eurjchem-1701	158	22	)	)	PUNCT
eurjchem-1701	158	23	,	,	PUNCT
eurjchem-1701	158	24	250	250	NUM
eurjchem-1701	158	25	(	(	PUNCT
eurjchem-1701	158	26	50	50	NUM
eurjchem-1701	158	27	)	)	PUNCT
eurjchem-1701	158	28	,	,	PUNCT
eurjchem-1701	158	29	173	173	NUM
eurjchem-1701	158	30	(	(	PUNCT
eurjchem-1701	158	31	55	55	NUM
eurjchem-1701	158	32	)	)	PUNCT
eurjchem-1701	158	33	,	,	PUNCT
eurjchem-1701	158	34	160	160	NUM
eurjchem-1701	158	35	(	(	PUNCT
eurjchem-1701	158	36	50	50	NUM
eurjchem-1701	158	37	)	)	PUNCT
eurjchem-1701	158	38	,	,	PUNCT
eurjchem-1701	158	39	112	112	NUM
eurjchem-1701	158	40	(	(	PUNCT
eurjchem-1701	158	41	60	60	NUM
eurjchem-1701	158	42	)	)	PUNCT
eurjchem-1701	158	43	.	.	PUNCT
eurjchem-1701	159	1	anal	anal	PROPN
eurjchem-1701	159	2	.	.	PUNCT
eurjchem-1701	159	3	calcd	calcd	NOUN
eurjchem-1701	159	4	.	.	PUNCT
eurjchem-1701	160	1	for	for	ADP
eurjchem-1701	160	2	c12h8n4os2	c12h8n4os2	NOUN
eurjchem-1701	160	3	:	:	PUNCT
eurjchem-1701	160	4	c	c	X
eurjchem-1701	160	5	,	,	PUNCT
eurjchem-1701	160	6	49.98	49.98	NUM
eurjchem-1701	160	7	;	;	PUNCT
eurjchem-1701	160	8	h	h	NOUN
eurjchem-1701	160	9	,	,	PUNCT
eurjchem-1701	160	10	2.80	2.80	NUM
eurjchem-1701	160	11	;	;	PUNCT
eurjchem-1701	160	12	n	n	CCONJ
eurjchem-1701	160	13	,	,	PUNCT
eurjchem-1701	160	14	19.43	19.43	NUM
eurjchem-1701	160	15	.	.	PUNCT
eurjchem-1701	160	16	found	find	VERB
eurjchem-1701	160	17	:	:	PUNCT
eurjchem-1701	161	1	c	c	X
eurjchem-1701	161	2	,	,	PUNCT
eurjchem-1701	161	3	49.87	49.87	NUM
eurjchem-1701	161	4	;	;	PUNCT
eurjchem-1701	161	5	h	h	NOUN
eurjchem-1701	161	6	,	,	PUNCT
eurjchem-1701	161	7	2.69	2.69	NUM
eurjchem-1701	161	8	;	;	PUNCT
eurjchem-1701	161	9	n	n	CCONJ
eurjchem-1701	161	10	,	,	PUNCT
eurjchem-1701	161	11	19.38	19.38	NUM
eurjchem-1701	161	12	%	%	NOUN
eurjchem-1701	161	13	.	.	PUNCT
eurjchem-1701	162	1	2018	2018	NUM
eurjchem-1701	162	2	–	–	PUNCT
eurjchem-1701	162	3	european	european	ADJ
eurjchem-1701	162	4	journal	journal	NOUN
eurjchem-1701	162	5	of	of	ADP
eurjchem-1701	162	6	chemistry	chemistry	NOUN
eurjchem-1701	162	7	–	–	PUNCT
eurjchem-1701	162	8	cc	cc	NOUN
eurjchem-1701	162	9	by	by	ADP
eurjchem-1701	162	10	nc	nc	PROPN
eurjchem-1701	162	11	–	–	PUNCT
eurjchem-1701	162	12	doi	doi	NOUN
eurjchem-1701	162	13	:	:	PUNCT
eurjchem-1701	162	14	10.5155	10.5155	NUM
eurjchem-1701	162	15	/	/	SYM
eurjchem-1701	162	16	eurjchem.9.2.99	eurjchem.9.2.99	NUM
eurjchem-1701	162	17	-	-	PUNCT
eurjchem-1701	162	18	106.1701	106.1701	NUM
eurjchem-1701	162	19	102	102	NUM
eurjchem-1701	162	20	haggam	haggam	NOUN
eurjchem-1701	162	21	et	et	PROPN
eurjchem-1701	162	22	al	al	PROPN
eurjchem-1701	162	23	.	.	PUNCT
eurjchem-1701	162	24	/	/	SYM
eurjchem-1701	162	25	european	european	PROPN
eurjchem-1701	162	26	journal	journal	PROPN
eurjchem-1701	162	27	of	of	ADP
eurjchem-1701	162	28	chemistry	chemistry	NOUN
eurjchem-1701	162	29	9	9	NUM
eurjchem-1701	162	30	(	(	PUNCT
eurjchem-1701	162	31	2	2	NUM
eurjchem-1701	162	32	)	)	PUNCT
eurjchem-1701	162	33	(	(	PUNCT
eurjchem-1701	162	34	2018	2018	NUM
eurjchem-1701	162	35	)	)	PUNCT
eurjchem-1701	162	36	99	99	NUM
eurjchem-1701	162	37	-	-	SYM
eurjchem-1701	162	38	106	106	NUM
eurjchem-1701	162	39	1	1	NUM
eurjchem-1701	162	40	s	s	NOUN
eurjchem-1701	162	41	o	o	NOUN
eurjchem-1701	162	42	n	n	ADP
eurjchem-1701	162	43	c	c	NOUN
eurjchem-1701	162	44	s	s	NOUN
eurjchem-1701	162	45	ph	ph	NOUN
eurjchem-1701	162	46	n	n	PROPN
eurjchem-1701	162	47	h	h	NOUN
eurjchem-1701	162	48	nh3	nh3	PROPN
eurjchem-1701	162	49	cl	cl	PROPN
eurjchem-1701	162	50	dioxane	dioxane	NOUN
eurjchem-1701	162	51	/	/	SYM
eurjchem-1701	162	52	h2o	h2o	PROPN
eurjchem-1701	162	53	(	(	PUNCT
eurjchem-1701	162	54	1:1	1:1	NUM
eurjchem-1701	162	55	)	)	PUNCT
eurjchem-1701	162	56	stirring	stirring	NOUN
eurjchem-1701	162	57	/	/	SYM
eurjchem-1701	162	58	r.t	r.t	PROPN
eurjchem-1701	162	59	.	.	PROPN
eurjchem-1701	162	60	/	/	SYM
eurjchem-1701	162	61	1	1	NUM
eurjchem-1701	162	62	h	h	NOUN
eurjchem-1701	162	63	54	54	NUM
eurjchem-1701	162	64	%	%	NOUN
eurjchem-1701	162	65	5	5	NUM
eurjchem-1701	162	66	s	s	NOUN
eurjchem-1701	162	67	o	o	NOUN
eurjchem-1701	162	68	h	h	NOUN
eurjchem-1701	162	69	n	n	ADP
eurjchem-1701	162	70	n	n	NUM
eurjchem-1701	162	71	nh3	nh3	NOUN
eurjchem-1701	162	72	s	s	NOUN
eurjchem-1701	162	73	ph	ph	NOUN
eurjchem-1701	162	74	cl	cl	NOUN
eurjchem-1701	163	1	o	o	NOUN
eurjchem-1701	163	2	o	o	X
eurjchem-1701	163	3	o	o	X
eurjchem-1701	163	4	dmf	dmf	PROPN
eurjchem-1701	163	5	/	/	SYM
eurjchem-1701	163	6	tea	tea	NOUN
eurjchem-1701	163	7	reflux	reflux	NOUN
eurjchem-1701	163	8	2	2	NUM
eurjchem-1701	163	9	h	h	NOUN
eurjchem-1701	163	10	61	61	NUM
eurjchem-1701	163	11	%	%	NOUN
eurjchem-1701	163	12	s	s	PART
eurjchem-1701	163	13	o	o	NOUN
eurjchem-1701	163	14	n	n	CCONJ
eurjchem-1701	163	15	n	n	PROPN
eurjchem-1701	163	16	nh	nh	PROPN
eurjchem-1701	163	17	s	s	PART
eurjchem-1701	163	18	ph	ph	NOUN
eurjchem-1701	163	19	o	o	NOUN
eurjchem-1701	163	20	o6	o6	PROPN
eurjchem-1701	163	21	s	s	PART
eurjchem-1701	163	22	o	o	NOUN
eurjchem-1701	163	23	n	n	CCONJ
eurjchem-1701	163	24	n	n	PROPN
eurjchem-1701	163	25	nh2	nh2	PROPN
eurjchem-1701	163	26	s	s	PART
eurjchem-1701	163	27	ph	ph	NOUN
eurjchem-1701	163	28	ch2	ch2	PROPN
eurjchem-1701	163	29	c	c	PROPN
eurjchem-1701	163	30	o	o	PROPN
eurjchem-1701	164	1	oet	oet	PROPN
eurjchem-1701	164	2	s	s	PART
eurjchem-1701	164	3	o	o	NOUN
eurjchem-1701	164	4	n	n	ADP
eurjchem-1701	164	5	n	n	CCONJ
eurjchem-1701	164	6	n	n	NOUN
eurjchem-1701	164	7	s	s	NOUN
eurjchem-1701	164	8	ph	ph	NOUN
eurjchem-1701	165	1	oh	oh	INTJ
eurjchem-1701	165	2	7	7	NUM
eurjchem-1701	165	3	cl	cl	NOUN
eurjchem-1701	165	4	oet	oet	ADJ
eurjchem-1701	165	5	otea	otea	NOUN
eurjchem-1701	165	6	/	/	SYM
eurjchem-1701	165	7	etoh	etoh	PROPN
eurjchem-1701	165	8	reflux	reflux	NOUN
eurjchem-1701	165	9	6	6	NUM
eurjchem-1701	165	10	h	h	NOUN
eurjchem-1701	165	11	79	79	NUM
eurjchem-1701	165	12	%	%	NOUN
eurjchem-1701	165	13	naoet	naoet	ADJ
eurjchem-1701	165	14	/	/	SYM
eurjchem-1701	165	15	etoh	etoh	PROPN
eurjchem-1701	165	16	reflux	reflux	NOUN
eurjchem-1701	165	17	2	2	NUM
eurjchem-1701	165	18	h	h	NOUN
eurjchem-1701	165	19	95	95	NUM
eurjchem-1701	165	20	%	%	NOUN
eurjchem-1701	165	21	8	8	NUM
eurjchem-1701	165	22	s	s	PART
eurjchem-1701	165	23	hn	hn	PROPN
eurjchem-1701	165	24	n	n	PROPN
eurjchem-1701	165	25	n	n	NOUN
eurjchem-1701	165	26	s	s	NOUN
eurjchem-1701	165	27	ph	ph	NOUN
eurjchem-1701	165	28	scheme	scheme	NOUN
eurjchem-1701	165	29	2	2	NUM
eurjchem-1701	165	30	9	9	NUM
eurjchem-1701	165	31	s	s	NOUN
eurjchem-1701	165	32	o	o	NOUN
eurjchem-1701	165	33	n	n	CCONJ
eurjchem-1701	165	34	n	n	PROPN
eurjchem-1701	165	35	nh2	nh2	PROPN
eurjchem-1701	165	36	s	s	PART
eurjchem-1701	165	37	ph	ph	NOUN
eurjchem-1701	165	38	o	o	NOUN
eurjchem-1701	165	39	o	o	X
eurjchem-1701	166	1	o	o	X
eurjchem-1701	166	2	s	s	X
eurjchem-1701	166	3	o	o	X
eurjchem-1701	166	4	n	n	CCONJ
eurjchem-1701	166	5	n	n	PROPN
eurjchem-1701	166	6	nh	nh	PROPN
eurjchem-1701	166	7	s	s	PART
eurjchem-1701	166	8	ph	ph	PROPN
eurjchem-1701	166	9	o	o	NOUN
eurjchem-1701	166	10	cooh	cooh	NOUN
eurjchem-1701	166	11	10	10	NUM
eurjchem-1701	166	12	5	5	NUM
eurjchem-1701	166	13	s	s	NOUN
eurjchem-1701	166	14	o	o	NOUN
eurjchem-1701	166	15	h	h	NOUN
eurjchem-1701	166	16	n	n	ADP
eurjchem-1701	166	17	n	n	NUM
eurjchem-1701	166	18	nh3	nh3	NOUN
eurjchem-1701	166	19	s	s	NOUN
eurjchem-1701	166	20	ph	ph	NOUN
eurjchem-1701	166	21	cl	cl	NOUN
eurjchem-1701	167	1	o	o	NOUN
eurjchem-1701	167	2	o	o	X
eurjchem-1701	167	3	o	o	X
eurjchem-1701	167	4	dmf	dmf	PROPN
eurjchem-1701	167	5	/	/	SYM
eurjchem-1701	167	6	tea	tea	NOUN
eurjchem-1701	167	7	s	s	PART
eurjchem-1701	167	8	o	o	PROPN
eurjchem-1701	167	9	n	n	CCONJ
eurjchem-1701	167	10	n	n	PROPN
eurjchem-1701	167	11	nh	nh	PROPN
eurjchem-1701	167	12	s	s	PART
eurjchem-1701	168	1	ph	ph	NOUN
eurjchem-1701	168	2	o	o	NOUN
eurjchem-1701	168	3	o6	o6	NOUN
eurjchem-1701	168	4	h	h	PROPN
eurjchem-1701	168	5	h2o	h2o	PROPN
eurjchem-1701	168	6	scheme	scheme	NOUN
eurjchem-1701	168	7	3	3	NUM
eurjchem-1701	168	8	2.3.10	2.3.10	NOUN
eurjchem-1701	168	9	.	.	PUNCT
eurjchem-1701	169	1	synthesis	synthesis	NOUN
eurjchem-1701	169	2	of	of	ADP
eurjchem-1701	169	3	(	(	PUNCT
eurjchem-1701	169	4	3	3	NUM
eurjchem-1701	169	5	-	-	PUNCT
eurjchem-1701	169	6	mercapto-5-(pyridin-4	mercapto-5-(pyridin-4	NOUN
eurjchem-1701	169	7	-	-	PUNCT
eurjchem-1701	169	8	yl)-4h-1,2,4triazol-4	yl)-4h-1,2,4triazol-4	NOUN
eurjchem-1701	169	9	-	-	PUNCT
eurjchem-1701	169	10	yl)(thiophen-2	yl)(thiophen-2	NOUN
eurjchem-1701	169	11	-	-	NOUN
eurjchem-1701	169	12	yl)methanone	yl)methanone	NOUN
eurjchem-1701	169	13	(	(	PUNCT
eurjchem-1701	169	14	13	13	NUM
eurjchem-1701	169	15	)	)	PUNCT
eurjchem-1701	169	16	a	a	DET
eurjchem-1701	169	17	mixture	mixture	NOUN
eurjchem-1701	169	18	of	of	ADP
eurjchem-1701	169	19	n-(2	n-(2	PROPN
eurjchem-1701	169	20	-	-	PUNCT
eurjchem-1701	169	21	isonicotinoylhydrazinecarbonothioyl	isonicotinoylhydrazinecarbonothioyl	ADJ
eurjchem-1701	169	22	)	)	PUNCT
eurjchem-1701	169	23	thiophene-2	thiophene-2	NUM
eurjchem-1701	169	24	-	-	PUNCT
eurjchem-1701	169	25	carboxamide	carboxamide	NOUN
eurjchem-1701	169	26	(	(	PUNCT
eurjchem-1701	169	27	11	11	NUM
eurjchem-1701	169	28	)	)	PUNCT
eurjchem-1701	169	29	(	(	PUNCT
eurjchem-1701	169	30	1.20	1.20	NUM
eurjchem-1701	169	31	mol	mol	NOUN
eurjchem-1701	169	32	)	)	PUNCT
eurjchem-1701	169	33	and	and	CCONJ
eurjchem-1701	169	34	lead	lead	VERB
eurjchem-1701	169	35	acetate	acetate	NOUN
eurjchem-1701	169	36	(	(	PUNCT
eurjchem-1701	169	37	1.20	1.20	NUM
eurjchem-1701	169	38	mol	mol	NOUN
eurjchem-1701	169	39	)	)	PUNCT
eurjchem-1701	169	40	in	in	ADP
eurjchem-1701	169	41	acetic	acetic	ADJ
eurjchem-1701	169	42	acid	acid	NOUN
eurjchem-1701	169	43	(	(	PUNCT
eurjchem-1701	169	44	20	20	NUM
eurjchem-1701	169	45	ml	ml	NOUN
eurjchem-1701	169	46	)	)	PUNCT
eurjchem-1701	169	47	was	be	AUX
eurjchem-1701	169	48	heated	heat	VERB
eurjchem-1701	169	49	under	under	ADP
eurjchem-1701	169	50	reflux	reflux	NOUN
eurjchem-1701	169	51	for	for	ADP
eurjchem-1701	169	52	6	6	NUM
eurjchem-1701	169	53	h.	h.	NOUN
eurjchem-1701	169	54	the	the	DET
eurjchem-1701	169	55	reaction	reaction	NOUN
eurjchem-1701	169	56	mixture	mixture	NOUN
eurjchem-1701	169	57	was	be	AUX
eurjchem-1701	169	58	poured	pour	VERB
eurjchem-1701	169	59	into	into	ADP
eurjchem-1701	169	60	water	water	NOUN
eurjchem-1701	169	61	.	.	PUNCT
eurjchem-1701	170	1	the	the	DET
eurjchem-1701	170	2	formed	form	VERB
eurjchem-1701	170	3	precipitate	precipitate	NOUN
eurjchem-1701	170	4	was	be	AUX
eurjchem-1701	170	5	filtered	filter	VERB
eurjchem-1701	170	6	off	off	ADP
eurjchem-1701	170	7	,	,	PUNCT
eurjchem-1701	170	8	dried	dry	VERB
eurjchem-1701	170	9	and	and	CCONJ
eurjchem-1701	170	10	crystallized	crystallize	VERB
eurjchem-1701	170	11	from	from	ADP
eurjchem-1701	170	12	ethanol	ethanol	NOUN
eurjchem-1701	170	13	to	to	PART
eurjchem-1701	170	14	give	give	VERB
eurjchem-1701	170	15	compound	compound	NOUN
eurjchem-1701	170	16	13	13	NUM
eurjchem-1701	170	17	(	(	PUNCT
eurjchem-1701	170	18	scheme	scheme	NOUN
eurjchem-1701	170	19	4	4	NUM
eurjchem-1701	170	20	)	)	PUNCT
eurjchem-1701	170	21	.	.	PUNCT
eurjchem-1701	171	1	color	color	NOUN
eurjchem-1701	171	2	:	:	PUNCT
eurjchem-1701	171	3	grey	grey	PROPN
eurjchem-1701	171	4	.	.	PUNCT
eurjchem-1701	172	1	yield	yield	NOUN
eurjchem-1701	172	2	:	:	PUNCT
eurjchem-1701	172	3	83	83	NUM
eurjchem-1701	172	4	%	%	NOUN
eurjchem-1701	172	5	.	.	PUNCT
eurjchem-1701	173	1	m.p	m.p	PROPN
eurjchem-1701	173	2	.	.	PROPN
eurjchem-1701	173	3	:	:	PUNCT
eurjchem-1701	174	1	327	327	NUM
eurjchem-1701	174	2	-	-	SYM
eurjchem-1701	174	3	328	328	NUM
eurjchem-1701	174	4	°	°	NOUN
eurjchem-1701	174	5	c	c	NOUN
eurjchem-1701	174	6	.	.	PUNCT
eurjchem-1701	174	7	ft	ft	PROPN
eurjchem-1701	174	8	-	-	PUNCT
eurjchem-1701	174	9	ir	ir	PROPN
eurjchem-1701	174	10	(	(	PUNCT
eurjchem-1701	174	11	kbr	kbr	PROPN
eurjchem-1701	174	12	,	,	PUNCT
eurjchem-1701	174	13	ν	ν	PROPN
eurjchem-1701	174	14	,	,	PUNCT
eurjchem-1701	174	15	cm-1	cm-1	NUM
eurjchem-1701	174	16	):	):	PUNCT
eurjchem-1701	174	17	3108	3108	NUM
eurjchem-1701	174	18	(	(	PUNCT
eurjchem-1701	174	19	ch	ch	NOUN
eurjchem-1701	174	20	arom	arom	NOUN
eurjchem-1701	174	21	.	.	PUNCT
eurjchem-1701	174	22	)	)	PUNCT
eurjchem-1701	174	23	,	,	PUNCT
eurjchem-1701	174	24	1661	1661	NUM
eurjchem-1701	174	25	(	(	PUNCT
eurjchem-1701	174	26	c	c	NOUN
eurjchem-1701	174	27	=	=	NOUN
eurjchem-1701	174	28	o	o	NOUN
eurjchem-1701	174	29	)	)	PUNCT
eurjchem-1701	174	30	,	,	PUNCT
eurjchem-1701	174	31	1624	1624	NUM
eurjchem-1701	174	32	(	(	PUNCT
eurjchem-1701	174	33	c	c	NOUN
eurjchem-1701	174	34	=	=	SYM
eurjchem-1701	174	35	c	c	NOUN
eurjchem-1701	174	36	)	)	PUNCT
eurjchem-1701	174	37	.	.	PUNCT
eurjchem-1701	175	1	1h	1h	NUM
eurjchem-1701	175	2	nmr	nmr	NOUN
eurjchem-1701	175	3	(	(	PUNCT
eurjchem-1701	175	4	300	300	NUM
eurjchem-1701	175	5	mhz	mhz	NOUN
eurjchem-1701	175	6	,	,	PUNCT
eurjchem-1701	175	7	dmso	dmso	NOUN
eurjchem-1701	175	8	-	-	NOUN
eurjchem-1701	175	9	d6	d6	NOUN
eurjchem-1701	175	10	,	,	PUNCT
eurjchem-1701	175	11	δ	δ	PROPN
eurjchem-1701	175	12	,	,	PUNCT
eurjchem-1701	175	13	ppm	ppm	NOUN
eurjchem-1701	175	14	):	):	PUNCT
eurjchem-1701	175	15	8.727.27	8.727.27	PROPN
eurjchem-1701	175	16	(	(	PUNCT
eurjchem-1701	175	17	m	m	PROPN
eurjchem-1701	175	18	,	,	PUNCT
eurjchem-1701	175	19	7h	7h	PROPN
eurjchem-1701	175	20	,	,	PUNCT
eurjchem-1701	175	21	arh	arh	PROPN
eurjchem-1701	175	22	’s	’s	PART
eurjchem-1701	175	23	+	+	NUM
eurjchem-1701	175	24	thiophene	thiophene	NOUN
eurjchem-1701	175	25	protons	proton	NOUN
eurjchem-1701	175	26	)	)	PUNCT
eurjchem-1701	175	27	,	,	PUNCT
eurjchem-1701	175	28	13.08	13.08	NUM
eurjchem-1701	175	29	(	(	PUNCT
eurjchem-1701	175	30	s	s	PROPN
eurjchem-1701	175	31	,	,	PUNCT
eurjchem-1701	175	32	1h	1h	NUM
eurjchem-1701	175	33	,	,	PUNCT
eurjchem-1701	175	34	d2o	d2o	NOUN
eurjchem-1701	175	35	exchangeable	exchangeable	ADJ
eurjchem-1701	175	36	,	,	PUNCT
eurjchem-1701	175	37	sh	sh	PROPN
eurjchem-1701	175	38	)	)	PUNCT
eurjchem-1701	175	39	.	.	PUNCT
eurjchem-1701	176	1	13c	13c	NOUN
eurjchem-1701	176	2	nmr	nmr	NOUN
eurjchem-1701	176	3	(	(	PUNCT
eurjchem-1701	176	4	75.4	75.4	NUM
eurjchem-1701	176	5	mhz	mhz	NOUN
eurjchem-1701	176	6	,	,	PUNCT
eurjchem-1701	176	7	dmso	dmso	NOUN
eurjchem-1701	176	8	-	-	NOUN
eurjchem-1701	176	9	d6	d6	NOUN
eurjchem-1701	176	10	,	,	PUNCT
eurjchem-1701	176	11	δ	δ	PROPN
eurjchem-1701	176	12	,	,	PUNCT
eurjchem-1701	176	13	ppm	ppm	NUM
eurjchem-1701	176	14	):	):	PUNCT
eurjchem-1701	176	15	168.4	168.4	NUM
eurjchem-1701	176	16	(	(	PUNCT
eurjchem-1701	176	17	1c	1c	NOUN
eurjchem-1701	176	18	,	,	PUNCT
eurjchem-1701	176	19	c	c	NOUN
eurjchem-1701	176	20	=	=	SYM
eurjchem-1701	176	21	o	o	NOUN
eurjchem-1701	176	22	)	)	PUNCT
eurjchem-1701	176	23	,	,	PUNCT
eurjchem-1701	176	24	157.6	157.6	NUM
eurjchem-1701	176	25	,	,	PUNCT
eurjchem-1701	176	26	152.8	152.8	NUM
eurjchem-1701	176	27	(	(	PUNCT
eurjchem-1701	176	28	2c	2c	NUM
eurjchem-1701	176	29	,	,	PUNCT
eurjchem-1701	176	30	triazole	triazole	NOUN
eurjchem-1701	176	31	ring	ring	NOUN
eurjchem-1701	176	32	)	)	PUNCT
eurjchem-1701	176	33	,	,	PUNCT
eurjchem-1701	176	34	149.6	149.6	NUM
eurjchem-1701	176	35	,	,	PUNCT
eurjchem-1701	176	36	134.3	134.3	NUM
eurjchem-1701	176	37	,	,	PUNCT
eurjchem-1701	176	38	124.2	124.2	NUM
eurjchem-1701	176	39	,	,	PUNCT
eurjchem-1701	176	40	129.2	129.2	NUM
eurjchem-1701	176	41	,	,	PUNCT
eurjchem-1701	176	42	128.1	128.1	NUM
eurjchem-1701	176	43	,	,	PUNCT
eurjchem-1701	176	44	127.6	127.6	NUM
eurjchem-1701	176	45	,	,	PUNCT
eurjchem-1701	176	46	120.0	120.0	NUM
eurjchem-1701	176	47	(	(	PUNCT
eurjchem-1701	176	48	ar	ar	NOUN
eurjchem-1701	176	49	-	-	NOUN
eurjchem-1701	176	50	c	c	NOUN
eurjchem-1701	176	51	)	)	PUNCT
eurjchem-1701	176	52	.	.	PUNCT
eurjchem-1701	177	1	ms	ms	NOUN
eurjchem-1701	177	2	(	(	PUNCT
eurjchem-1701	177	3	ei	ei	PROPN
eurjchem-1701	177	4	,	,	PUNCT
eurjchem-1701	177	5	m	m	PROPN
eurjchem-1701	177	6	/	/	SYM
eurjchem-1701	177	7	z	z	PROPN
eurjchem-1701	177	8	(	(	PUNCT
eurjchem-1701	177	9	%	%	NOUN
eurjchem-1701	177	10	)	)	PUNCT
eurjchem-1701	177	11	):	):	PUNCT
eurjchem-1701	177	12	288	288	NUM
eurjchem-1701	177	13	(	(	PUNCT
eurjchem-1701	177	14	m+	m+	NUM
eurjchem-1701	177	15	,	,	PUNCT
eurjchem-1701	177	16	100	100	NUM
eurjchem-1701	177	17	)	)	PUNCT
eurjchem-1701	177	18	,	,	PUNCT
eurjchem-1701	177	19	259	259	NUM
eurjchem-1701	177	20	(	(	PUNCT
eurjchem-1701	177	21	55	55	NUM
eurjchem-1701	177	22	)	)	PUNCT
eurjchem-1701	177	23	,	,	PUNCT
eurjchem-1701	177	24	193	193	NUM
eurjchem-1701	177	25	(	(	PUNCT
eurjchem-1701	177	26	15	15	NUM
eurjchem-1701	177	27	)	)	PUNCT
eurjchem-1701	177	28	,	,	PUNCT
eurjchem-1701	177	29	127	127	NUM
eurjchem-1701	177	30	(	(	PUNCT
eurjchem-1701	177	31	20	20	NUM
eurjchem-1701	177	32	)	)	PUNCT
eurjchem-1701	177	33	,	,	PUNCT
eurjchem-1701	177	34	110	110	NUM
eurjchem-1701	177	35	(	(	PUNCT
eurjchem-1701	177	36	95	95	NUM
eurjchem-1701	177	37	)	)	PUNCT
eurjchem-1701	177	38	,	,	PUNCT
eurjchem-1701	177	39	63	63	NUM
eurjchem-1701	177	40	(	(	PUNCT
eurjchem-1701	177	41	15	15	NUM
eurjchem-1701	177	42	)	)	PUNCT
eurjchem-1701	177	43	.	.	PUNCT
eurjchem-1701	178	1	anal	anal	PROPN
eurjchem-1701	178	2	.	.	PUNCT
eurjchem-1701	178	3	calcd	calcd	NOUN
eurjchem-1701	178	4	.	.	PUNCT
eurjchem-1701	179	1	for	for	ADP
eurjchem-1701	179	2	c12h8n4os2	c12h8n4os2	NOUN
eurjchem-1701	179	3	:	:	PUNCT
eurjchem-1701	179	4	c	c	X
eurjchem-1701	179	5	,	,	PUNCT
eurjchem-1701	179	6	49.98	49.98	NUM
eurjchem-1701	179	7	;	;	PUNCT
eurjchem-1701	179	8	h	h	NOUN
eurjchem-1701	179	9	,	,	PUNCT
eurjchem-1701	179	10	2.80	2.80	NUM
eurjchem-1701	179	11	;	;	PUNCT
eurjchem-1701	179	12	n	n	CCONJ
eurjchem-1701	179	13	,	,	PUNCT
eurjchem-1701	179	14	19.43	19.43	NUM
eurjchem-1701	179	15	.	.	PUNCT
eurjchem-1701	179	16	found	find	VERB
eurjchem-1701	179	17	:	:	PUNCT
eurjchem-1701	180	1	c	c	X
eurjchem-1701	180	2	,	,	PUNCT
eurjchem-1701	180	3	49.91	49.91	NUM
eurjchem-1701	180	4	;	;	PUNCT
eurjchem-1701	180	5	h	h	X
eurjchem-1701	180	6	,	,	PUNCT
eurjchem-1701	180	7	2.75	2.75	NUM
eurjchem-1701	180	8	;	;	PUNCT
eurjchem-1701	180	9	n	n	CCONJ
eurjchem-1701	180	10	,	,	PUNCT
eurjchem-1701	180	11	19.35	19.35	NUM
eurjchem-1701	180	12	%	%	NOUN
eurjchem-1701	180	13	.	.	PUNCT
eurjchem-1701	181	1	2.3.11	2.3.11	X
eurjchem-1701	181	2	.	.	PUNCT
eurjchem-1701	182	1	synthesis	synthesis	NOUN
eurjchem-1701	182	2	of	of	ADP
eurjchem-1701	182	3	5-(pyridin-4	5-(pyridin-4	NUM
eurjchem-1701	182	4	-	-	ADJ
eurjchem-1701	182	5	yl)-2h-1,2,4	yl)-2h-1,2,4	NOUN
eurjchem-1701	182	6	-	-	PUNCT
eurjchem-1701	182	7	triazole3(4h)-thione	triazole3(4h)-thione	NOUN
eurjchem-1701	182	8	(	(	PUNCT
eurjchem-1701	182	9	14	14	NUM
eurjchem-1701	182	10	)	)	PUNCT
eurjchem-1701	182	11	a	a	DET
eurjchem-1701	182	12	mixture	mixture	NOUN
eurjchem-1701	182	13	of	of	ADP
eurjchem-1701	182	14	n-(2	n-(2	PROPN
eurjchem-1701	182	15	-	-	PUNCT
eurjchem-1701	182	16	isonicotinoylhydrazinecarbonothioyl	isonicotinoylhydrazinecarbonothioyl	ADJ
eurjchem-1701	182	17	)	)	PUNCT
eurjchem-1701	182	18	thiophene-2	thiophene-2	NUM
eurjchem-1701	182	19	-	-	PUNCT
eurjchem-1701	182	20	carboxamide	carboxamide	NOUN
eurjchem-1701	182	21	(	(	PUNCT
eurjchem-1701	182	22	11	11	NUM
eurjchem-1701	182	23	)	)	PUNCT
eurjchem-1701	182	24	(	(	PUNCT
eurjchem-1701	182	25	1.20	1.20	NUM
eurjchem-1701	182	26	mol	mol	NOUN
eurjchem-1701	182	27	)	)	PUNCT
eurjchem-1701	182	28	and	and	CCONJ
eurjchem-1701	182	29	potassium	potassium	NOUN
eurjchem-1701	182	30	hydroxide	hydroxide	NOUN
eurjchem-1701	182	31	(	(	PUNCT
eurjchem-1701	182	32	1.20	1.20	NUM
eurjchem-1701	182	33	mol	mol	NOUN
eurjchem-1701	182	34	)	)	PUNCT
eurjchem-1701	182	35	in	in	ADP
eurjchem-1701	182	36	ethanol	ethanol	NOUN
eurjchem-1701	182	37	(	(	PUNCT
eurjchem-1701	182	38	20	20	NUM
eurjchem-1701	182	39	ml	ml	NOUN
eurjchem-1701	182	40	)	)	PUNCT
eurjchem-1701	182	41	was	be	AUX
eurjchem-1701	182	42	heated	heat	VERB
eurjchem-1701	182	43	under	under	ADP
eurjchem-1701	182	44	reflux	reflux	NOUN
eurjchem-1701	182	45	for	for	ADP
eurjchem-1701	182	46	6	6	NUM
eurjchem-1701	182	47	h.	h.	NOUN
eurjchem-1701	182	48	2018	2018	NUM
eurjchem-1701	182	49	–	–	PUNCT
eurjchem-1701	182	50	european	european	ADJ
eurjchem-1701	182	51	journal	journal	NOUN
eurjchem-1701	182	52	of	of	ADP
eurjchem-1701	182	53	chemistry	chemistry	NOUN
eurjchem-1701	182	54	–	–	PUNCT
eurjchem-1701	182	55	cc	cc	NOUN
eurjchem-1701	182	56	by	by	ADP
eurjchem-1701	182	57	nc	nc	PROPN
eurjchem-1701	182	58	–	–	PUNCT
eurjchem-1701	182	59	doi	doi	NOUN
eurjchem-1701	182	60	:	:	PUNCT
eurjchem-1701	182	61	10.5155	10.5155	NUM
eurjchem-1701	182	62	/	/	SYM
eurjchem-1701	182	63	eurjchem.9.2.99	eurjchem.9.2.99	NUM
eurjchem-1701	182	64	-	-	PUNCT
eurjchem-1701	182	65	106.1701	106.1701	NUM
eurjchem-1701	182	66	haggam	haggam	NOUN
eurjchem-1701	182	67	et	et	PROPN
eurjchem-1701	182	68	al	al	PROPN
eurjchem-1701	182	69	.	.	PUNCT
eurjchem-1701	182	70	/	/	SYM
eurjchem-1701	182	71	european	european	PROPN
eurjchem-1701	182	72	journal	journal	PROPN
eurjchem-1701	182	73	of	of	ADP
eurjchem-1701	182	74	chemistry	chemistry	NOUN
eurjchem-1701	182	75	9	9	NUM
eurjchem-1701	182	76	(	(	PUNCT
eurjchem-1701	182	77	2	2	NUM
eurjchem-1701	182	78	)	)	PUNCT
eurjchem-1701	182	79	(	(	PUNCT
eurjchem-1701	182	80	2018	2018	NUM
eurjchem-1701	182	81	)	)	PUNCT
eurjchem-1701	182	82	99	99	NUM
eurjchem-1701	182	83	-	-	SYM
eurjchem-1701	182	84	106	106	NUM
eurjchem-1701	182	85	103	103	NUM
eurjchem-1701	182	86	1	1	NUM
eurjchem-1701	182	87	s	s	NOUN
eurjchem-1701	182	88	o	o	NOUN
eurjchem-1701	183	1	n	n	ADP
eurjchem-1701	183	2	c	c	NOUN
eurjchem-1701	183	3	s	s	VERB
eurjchem-1701	183	4	dioxane	dioxane	NOUN
eurjchem-1701	183	5	/	/	SYM
eurjchem-1701	183	6	stirring	stirring	NOUN
eurjchem-1701	183	7	/	/	SYM
eurjchem-1701	183	8	r.t	r.t	PROPN
eurjchem-1701	183	9	.	.	PROPN
eurjchem-1701	183	10	1	1	NUM
eurjchem-1701	183	11	h	h	NOUN
eurjchem-1701	183	12	koh	koh	PROPN
eurjchem-1701	183	13	/	/	SYM
eurjchem-1701	183	14	etoh	etoh	PROPN
eurjchem-1701	183	15	reflux	reflux	NOUN
eurjchem-1701	183	16	6	6	NUM
eurjchem-1701	183	17	h	h	NOUN
eurjchem-1701	183	18	95	95	NUM
eurjchem-1701	183	19	%	%	NOUN
eurjchem-1701	184	1	n	n	PRON
eurjchem-1701	184	2	h	h	NOUN
eurjchem-1701	184	3	h2n	h2n	PROPN
eurjchem-1701	184	4	o	o	PROPN
eurjchem-1701	185	1	n	n	NOUN
eurjchem-1701	185	2	s	s	NOUN
eurjchem-1701	185	3	o	o	NOUN
eurjchem-1701	185	4	12	12	NUM
eurjchem-1701	185	5	13	13	NUM
eurjchem-1701	185	6	s	s	NOUN
eurjchem-1701	185	7	o	o	NOUN
eurjchem-1701	185	8	h	h	NOUN
eurjchem-1701	185	9	n	n	ADP
eurjchem-1701	185	10	n	n	CCONJ
eurjchem-1701	185	11	n	n	PROPN
eurjchem-1701	185	12	s	s	PART
eurjchem-1701	185	13	n	n	CCONJ
eurjchem-1701	185	14	n	n	CCONJ
eurjchem-1701	185	15	n	n	CCONJ
eurjchem-1701	185	16	n	n	CCONJ
eurjchem-1701	185	17	n	n	NOUN
eurjchem-1701	185	18	hs	hs	ADV
eurjchem-1701	185	19	pb(ch3coo)2	pb(ch3coo)2	PROPN
eurjchem-1701	185	20	/	/	SYM
eurjchem-1701	185	21	acoh	acoh	ADJ
eurjchem-1701	185	22	reflux	reflux	NOUN
eurjchem-1701	185	23	6	6	NUM
eurjchem-1701	185	24	h	h	NOUN
eurjchem-1701	185	25	s	s	PART
eurjchem-1701	185	26	o	o	NOUN
eurjchem-1701	185	27	n	n	CCONJ
eurjchem-1701	185	28	n	n	PROPN
eurjchem-1701	185	29	h	h	NOUN
eurjchem-1701	185	30	n	n	CCONJ
eurjchem-1701	185	31	n	n	PROPN
eurjchem-1701	185	32	s	s	PROPN
eurjchem-1701	185	33	hyd	hyd	NOUN
eurjchem-1701	185	34	.	.	PUNCT
eurjchem-1701	186	1	hn	hn	PROPN
eurjchem-1701	186	2	n	n	PROPN
eurjchem-1701	186	3	h	h	NOUN
eurjchem-1701	186	4	n	n	CCONJ
eurjchem-1701	186	5	n	n	PROPN
eurjchem-1701	186	6	s	s	PART
eurjchem-1701	186	7	14	14	NUM
eurjchem-1701	186	8	58	58	NUM
eurjchem-1701	186	9	%	%	NOUN
eurjchem-1701	187	1	11	11	NUM
eurjchem-1701	187	2	s	s	NOUN
eurjchem-1701	187	3	o	o	NOUN
eurjchem-1701	187	4	h	h	NOUN
eurjchem-1701	187	5	n	n	NOUN
eurjchem-1701	187	6	h	h	NOUN
eurjchem-1701	187	7	n	n	CCONJ
eurjchem-1701	187	8	n	n	NOUN
eurjchem-1701	187	9	h	h	NOUN
eurjchem-1701	187	10	s	s	NOUN
eurjchem-1701	187	11	o	o	X
eurjchem-1701	187	12	n	n	CCONJ
eurjchem-1701	187	13	h2so4	h2so4	PROPN
eurjchem-1701	187	14	/	/	SYM
eurjchem-1701	187	15	etoh	etoh	PROPN
eurjchem-1701	187	16	reflux	reflux	NOUN
eurjchem-1701	187	17	6	6	NUM
eurjchem-1701	187	18	h	h	NOUN
eurjchem-1701	187	19	83	83	NUM
eurjchem-1701	187	20	%	%	NOUN
eurjchem-1701	187	21	-h2o	-h2o	NOUN
eurjchem-1701	187	22	93	93	NUM
eurjchem-1701	187	23	%	%	NOUN
eurjchem-1701	187	24	scheme	scheme	NOUN
eurjchem-1701	187	25	4	4	NUM
eurjchem-1701	187	26	the	the	DET
eurjchem-1701	187	27	reaction	reaction	NOUN
eurjchem-1701	187	28	mixture	mixture	NOUN
eurjchem-1701	187	29	was	be	AUX
eurjchem-1701	187	30	poured	pour	VERB
eurjchem-1701	187	31	into	into	ADP
eurjchem-1701	187	32	water	water	NOUN
eurjchem-1701	187	33	.	.	PUNCT
eurjchem-1701	188	1	the	the	DET
eurjchem-1701	188	2	formed	form	VERB
eurjchem-1701	188	3	precipitate	precipitate	NOUN
eurjchem-1701	188	4	was	be	AUX
eurjchem-1701	188	5	filtered	filter	VERB
eurjchem-1701	188	6	off	off	ADP
eurjchem-1701	188	7	,	,	PUNCT
eurjchem-1701	188	8	dried	dry	VERB
eurjchem-1701	188	9	and	and	CCONJ
eurjchem-1701	188	10	crystallized	crystallize	VERB
eurjchem-1701	188	11	from	from	ADP
eurjchem-1701	188	12	ethanol	ethanol	NOUN
eurjchem-1701	188	13	to	to	PART
eurjchem-1701	188	14	give	give	VERB
eurjchem-1701	188	15	compound	compound	NOUN
eurjchem-1701	188	16	14	14	NUM
eurjchem-1701	188	17	(	(	PUNCT
eurjchem-1701	188	18	scheme	scheme	NOUN
eurjchem-1701	188	19	4	4	NUM
eurjchem-1701	188	20	)	)	PUNCT
eurjchem-1701	188	21	.	.	PUNCT
eurjchem-1701	189	1	color	color	NOUN
eurjchem-1701	189	2	:	:	PUNCT
eurjchem-1701	189	3	yellow	yellow	ADJ
eurjchem-1701	189	4	.	.	PUNCT
eurjchem-1701	190	1	yield	yield	NOUN
eurjchem-1701	190	2	:	:	PUNCT
eurjchem-1701	190	3	93	93	NUM
eurjchem-1701	190	4	%	%	NOUN
eurjchem-1701	190	5	.	.	PUNCT
eurjchem-1701	191	1	m.p	m.p	PROPN
eurjchem-1701	191	2	.	.	PROPN
eurjchem-1701	191	3	:	:	PUNCT
eurjchem-1701	192	1	318	318	NUM
eurjchem-1701	192	2	-	-	SYM
eurjchem-1701	192	3	319	319	NUM
eurjchem-1701	192	4	°	°	NUM
eurjchem-1701	192	5	c	c	NOUN
eurjchem-1701	192	6	.	.	PUNCT
eurjchem-1701	193	1	ft	ft	PROPN
eurjchem-1701	193	2	-	-	PUNCT
eurjchem-1701	193	3	ir	ir	PROPN
eurjchem-1701	193	4	(	(	PUNCT
eurjchem-1701	193	5	kbr	kbr	PROPN
eurjchem-1701	193	6	,	,	PUNCT
eurjchem-1701	193	7	ν	ν	PROPN
eurjchem-1701	193	8	,	,	PUNCT
eurjchem-1701	193	9	cm-1	cm-1	NUM
eurjchem-1701	193	10	):	):	PUNCT
eurjchem-1701	193	11	3445	3445	NUM
eurjchem-1701	193	12	(	(	PUNCT
eurjchem-1701	193	13	nh	nh	NOUN
eurjchem-1701	193	14	)	)	PUNCT
eurjchem-1701	193	15	,	,	PUNCT
eurjchem-1701	193	16	3087	3087	NUM
eurjchem-1701	193	17	(	(	PUNCT
eurjchem-1701	193	18	ch	ch	NOUN
eurjchem-1701	193	19	arom	arom	NOUN
eurjchem-1701	193	20	.	.	PUNCT
eurjchem-1701	193	21	)	)	PUNCT
eurjchem-1701	193	22	,	,	PUNCT
eurjchem-1701	193	23	1648	1648	NUM
eurjchem-1701	193	24	(	(	PUNCT
eurjchem-1701	193	25	c	c	NOUN
eurjchem-1701	193	26	=	=	SYM
eurjchem-1701	193	27	n	n	NUM
eurjchem-1701	193	28	)	)	PUNCT
eurjchem-1701	193	29	.	.	PUNCT
eurjchem-1701	194	1	1h	1h	NUM
eurjchem-1701	194	2	nmr	nmr	NOUN
eurjchem-1701	194	3	(	(	PUNCT
eurjchem-1701	194	4	300	300	NUM
eurjchem-1701	194	5	mhz	mhz	NOUN
eurjchem-1701	194	6	,	,	PUNCT
eurjchem-1701	194	7	dmso	dmso	NOUN
eurjchem-1701	194	8	-	-	NOUN
eurjchem-1701	194	9	d6	d6	NOUN
eurjchem-1701	194	10	,	,	PUNCT
eurjchem-1701	194	11	δ	δ	PROPN
eurjchem-1701	194	12	,	,	PUNCT
eurjchem-1701	194	13	ppm	ppm	NUM
eurjchem-1701	194	14	):	):	PUNCT
eurjchem-1701	194	15	8.46	8.46	NUM
eurjchem-1701	194	16	-	-	SYM
eurjchem-1701	194	17	7.15	7.15	NUM
eurjchem-1701	194	18	(	(	PUNCT
eurjchem-1701	194	19	m	m	PROPN
eurjchem-1701	194	20	,	,	PUNCT
eurjchem-1701	194	21	4h	4h	NUM
eurjchem-1701	194	22	,	,	PUNCT
eurjchem-1701	194	23	arh	arh	PROPN
eurjchem-1701	194	24	’s	’s	PART
eurjchem-1701	194	25	)	)	PUNCT
eurjchem-1701	194	26	,	,	PUNCT
eurjchem-1701	194	27	8.97	8.97	NUM
eurjchem-1701	194	28	(	(	PUNCT
eurjchem-1701	194	29	s	s	PROPN
eurjchem-1701	194	30	,	,	PUNCT
eurjchem-1701	194	31	1h	1h	NUM
eurjchem-1701	194	32	,	,	PUNCT
eurjchem-1701	194	33	d2o	d2o	NOUN
eurjchem-1701	194	34	exchangeable	exchangeable	ADJ
eurjchem-1701	194	35	,	,	PUNCT
eurjchem-1701	194	36	nh	nh	PROPN
eurjchem-1701	194	37	)	)	PUNCT
eurjchem-1701	194	38	,	,	PUNCT
eurjchem-1701	194	39	8.98	8.98	NUM
eurjchem-1701	194	40	(	(	PUNCT
eurjchem-1701	194	41	s	s	PROPN
eurjchem-1701	194	42	,	,	PUNCT
eurjchem-1701	194	43	1h	1h	NUM
eurjchem-1701	194	44	,	,	PUNCT
eurjchem-1701	194	45	d2o	d2o	NOUN
eurjchem-1701	194	46	exchangeable	exchangeable	ADJ
eurjchem-1701	194	47	,	,	PUNCT
eurjchem-1701	194	48	nh	nh	PROPN
eurjchem-1701	194	49	)	)	PUNCT
eurjchem-1701	194	50	.	.	PUNCT
eurjchem-1701	195	1	13c	13c	NOUN
eurjchem-1701	195	2	nmr	nmr	NOUN
eurjchem-1701	195	3	(	(	PUNCT
eurjchem-1701	195	4	75.4	75.4	NUM
eurjchem-1701	195	5	mhz	mhz	NOUN
eurjchem-1701	195	6	,	,	PUNCT
eurjchem-1701	195	7	dmso	dmso	NOUN
eurjchem-1701	195	8	-	-	NOUN
eurjchem-1701	195	9	d6	d6	NOUN
eurjchem-1701	195	10	,	,	PUNCT
eurjchem-1701	195	11	δ	δ	PROPN
eurjchem-1701	195	12	,	,	PUNCT
eurjchem-1701	195	13	ppm	ppm	NOUN
eurjchem-1701	195	14	):	):	PUNCT
eurjchem-1701	195	15	169.6	169.6	NUM
eurjchem-1701	195	16	,	,	PUNCT
eurjchem-1701	195	17	151.5	151.5	NUM
eurjchem-1701	195	18	(	(	PUNCT
eurjchem-1701	195	19	2c	2c	NUM
eurjchem-1701	195	20	,	,	PUNCT
eurjchem-1701	195	21	triazole	triazole	NOUN
eurjchem-1701	195	22	ring	ring	NOUN
eurjchem-1701	195	23	)	)	PUNCT
eurjchem-1701	195	24	,	,	PUNCT
eurjchem-1701	195	25	148.1	148.1	NUM
eurjchem-1701	195	26	,	,	PUNCT
eurjchem-1701	195	27	134.8	134.8	NUM
eurjchem-1701	195	28	,	,	PUNCT
eurjchem-1701	195	29	123.0	123.0	NUM
eurjchem-1701	195	30	(	(	PUNCT
eurjchem-1701	195	31	ar	ar	NOUN
eurjchem-1701	195	32	-	-	NOUN
eurjchem-1701	195	33	c	c	NOUN
eurjchem-1701	195	34	)	)	PUNCT
eurjchem-1701	195	35	.	.	PUNCT
eurjchem-1701	196	1	ms	ms	NOUN
eurjchem-1701	196	2	(	(	PUNCT
eurjchem-1701	196	3	ei	ei	PROPN
eurjchem-1701	196	4	,	,	PUNCT
eurjchem-1701	196	5	m	m	PROPN
eurjchem-1701	196	6	/	/	SYM
eurjchem-1701	196	7	z	z	PROPN
eurjchem-1701	196	8	(	(	PUNCT
eurjchem-1701	196	9	%	%	NOUN
eurjchem-1701	196	10	)	)	PUNCT
eurjchem-1701	196	11	):	):	PUNCT
eurjchem-1701	196	12	178	178	NUM
eurjchem-1701	196	13	(	(	PUNCT
eurjchem-1701	196	14	m+	m+	NUM
eurjchem-1701	196	15	,	,	PUNCT
eurjchem-1701	196	16	10	10	NUM
eurjchem-1701	196	17	)	)	PUNCT
eurjchem-1701	196	18	,	,	PUNCT
eurjchem-1701	196	19	127	127	NUM
eurjchem-1701	196	20	(	(	PUNCT
eurjchem-1701	196	21	60	60	NUM
eurjchem-1701	196	22	)	)	PUNCT
eurjchem-1701	196	23	,	,	PUNCT
eurjchem-1701	196	24	110	110	NUM
eurjchem-1701	196	25	(	(	PUNCT
eurjchem-1701	196	26	100	100	NUM
eurjchem-1701	196	27	)	)	PUNCT
eurjchem-1701	196	28	,	,	PUNCT
eurjchem-1701	196	29	82	82	NUM
eurjchem-1701	196	30	(	(	PUNCT
eurjchem-1701	196	31	15	15	NUM
eurjchem-1701	196	32	)	)	PUNCT
eurjchem-1701	196	33	,	,	PUNCT
eurjchem-1701	196	34	56	56	NUM
eurjchem-1701	196	35	(	(	PUNCT
eurjchem-1701	196	36	35	35	NUM
eurjchem-1701	196	37	)	)	PUNCT
eurjchem-1701	196	38	.	.	PUNCT
eurjchem-1701	197	1	anal	anal	PROPN
eurjchem-1701	197	2	.	.	PUNCT
eurjchem-1701	197	3	calcd	calcd	NOUN
eurjchem-1701	197	4	.	.	PUNCT
eurjchem-1701	198	1	for	for	ADP
eurjchem-1701	198	2	c7h6n4s	c7h6n4s	PROPN
eurjchem-1701	198	3	:	:	PUNCT
eurjchem-1701	198	4	c	c	NOUN
eurjchem-1701	198	5	,	,	PUNCT
eurjchem-1701	198	6	47.18	47.18	NUM
eurjchem-1701	198	7	;	;	PUNCT
eurjchem-1701	198	8	h	h	NOUN
eurjchem-1701	198	9	,	,	PUNCT
eurjchem-1701	198	10	3.39	3.39	NUM
eurjchem-1701	198	11	;	;	PUNCT
eurjchem-1701	198	12	n	n	CCONJ
eurjchem-1701	198	13	,	,	PUNCT
eurjchem-1701	198	14	31.44	31.44	NUM
eurjchem-1701	198	15	.	.	PUNCT
eurjchem-1701	198	16	found	find	VERB
eurjchem-1701	198	17	:	:	PUNCT
eurjchem-1701	199	1	c	c	X
eurjchem-1701	199	2	,	,	PUNCT
eurjchem-1701	199	3	47.10	47.10	NUM
eurjchem-1701	199	4	;	;	PUNCT
eurjchem-1701	200	1	h	h	NOUN
eurjchem-1701	200	2	,	,	PUNCT
eurjchem-1701	200	3	3.26	3.26	NUM
eurjchem-1701	200	4	;	;	PUNCT
eurjchem-1701	200	5	n	n	CCONJ
eurjchem-1701	200	6	,	,	PUNCT
eurjchem-1701	200	7	31.33	31.33	NUM
eurjchem-1701	200	8	%	%	NOUN
eurjchem-1701	200	9	.	.	PUNCT
eurjchem-1701	201	1	2.3.12	2.3.12	X
eurjchem-1701	201	2	.	.	X
eurjchem-1701	202	1	synthesis	synthesis	NOUN
eurjchem-1701	202	2	of	of	ADP
eurjchem-1701	202	3	ethyl	ethyl	PROPN
eurjchem-1701	202	4	2-(3-(thiophene-2	2-(3-(thiophene-2	NUM
eurjchem-1701	202	5	-	-	PUNCT
eurjchem-1701	202	6	carbonyl)thioureido)-4,5,6,7	carbonyl)thioureido)-4,5,6,7	NOUN
eurjchem-1701	202	7	-	-	PUNCT
eurjchem-1701	202	8	tetrahydrobenzo[b]thiophene-3	tetrahydrobenzo[b]thiophene-3	NOUN
eurjchem-1701	202	9	-	-	PUNCT
eurjchem-1701	202	10	carboxylate	carboxylate	NOUN
eurjchem-1701	202	11	(	(	PUNCT
eurjchem-1701	202	12	15	15	NUM
eurjchem-1701	202	13	)	)	PUNCT
eurjchem-1701	202	14	a	a	DET
eurjchem-1701	202	15	mixture	mixture	NOUN
eurjchem-1701	202	16	of	of	ADP
eurjchem-1701	202	17	thiophene-2	thiophene-2	NOUN
eurjchem-1701	202	18	-	-	PUNCT
eurjchem-1701	202	19	carbonylisothiocyanate	carbonylisothiocyanate	NOUN
eurjchem-1701	202	20	(	(	PUNCT
eurjchem-1701	202	21	1	1	NUM
eurjchem-1701	202	22	)	)	PUNCT
eurjchem-1701	202	23	(	(	PUNCT
eurjchem-1701	202	24	3.3	3.3	NUM
eurjchem-1701	202	25	mol	mol	NOUN
eurjchem-1701	202	26	)	)	PUNCT
eurjchem-1701	202	27	and	and	CCONJ
eurjchem-1701	202	28	ethyl	ethyl	PROPN
eurjchem-1701	202	29	2	2	NUM
eurjchem-1701	202	30	-	-	PUNCT
eurjchem-1701	202	31	amino-4,5,6,7	amino-4,5,6,7	ADP
eurjchem-1701	202	32	-	-	PUNCT
eurjchem-1701	202	33	tetrahydrobenzo[b]thiophene3	tetrahydrobenzo[b]thiophene3	NOUN
eurjchem-1701	202	34	-	-	PUNCT
eurjchem-1701	202	35	carboxylate	carboxylate	NOUN
eurjchem-1701	202	36	(	(	PUNCT
eurjchem-1701	202	37	3.3	3.3	NUM
eurjchem-1701	202	38	mol	mol	NOUN
eurjchem-1701	202	39	)	)	PUNCT
eurjchem-1701	202	40	in	in	ADP
eurjchem-1701	202	41	dioxane	dioxane	NOUN
eurjchem-1701	202	42	(	(	PUNCT
eurjchem-1701	202	43	50	50	NUM
eurjchem-1701	202	44	ml	ml	NOUN
eurjchem-1701	202	45	)	)	PUNCT
eurjchem-1701	202	46	was	be	AUX
eurjchem-1701	202	47	heated	heat	VERB
eurjchem-1701	202	48	under	under	ADP
eurjchem-1701	202	49	reflux	reflux	NOUN
eurjchem-1701	202	50	for	for	ADP
eurjchem-1701	202	51	1	1	NUM
eurjchem-1701	202	52	h.	h.	NOUN
eurjchem-1701	202	53	the	the	DET
eurjchem-1701	202	54	reaction	reaction	NOUN
eurjchem-1701	202	55	mixture	mixture	NOUN
eurjchem-1701	202	56	was	be	AUX
eurjchem-1701	202	57	poured	pour	VERB
eurjchem-1701	202	58	into	into	ADP
eurjchem-1701	202	59	water	water	NOUN
eurjchem-1701	202	60	.	.	PUNCT
eurjchem-1701	203	1	the	the	DET
eurjchem-1701	203	2	formed	form	VERB
eurjchem-1701	203	3	precipitate	precipitate	NOUN
eurjchem-1701	203	4	was	be	AUX
eurjchem-1701	203	5	filtered	filter	VERB
eurjchem-1701	203	6	off	off	ADP
eurjchem-1701	203	7	,	,	PUNCT
eurjchem-1701	203	8	washed	wash	VERB
eurjchem-1701	203	9	with	with	ADP
eurjchem-1701	203	10	water	water	NOUN
eurjchem-1701	203	11	,	,	PUNCT
eurjchem-1701	203	12	dried	dry	VERB
eurjchem-1701	203	13	and	and	CCONJ
eurjchem-1701	203	14	crystallized	crystallize	VERB
eurjchem-1701	203	15	from	from	ADP
eurjchem-1701	203	16	acetic	acetic	ADJ
eurjchem-1701	203	17	acid	acid	NOUN
eurjchem-1701	203	18	to	to	PART
eurjchem-1701	203	19	give	give	VERB
eurjchem-1701	203	20	compound	compound	NOUN
eurjchem-1701	203	21	15	15	NUM
eurjchem-1701	203	22	(	(	PUNCT
eurjchem-1701	203	23	scheme	scheme	NOUN
eurjchem-1701	203	24	5	5	NUM
eurjchem-1701	203	25	)	)	PUNCT
eurjchem-1701	203	26	.	.	PUNCT
eurjchem-1701	204	1	color	color	NOUN
eurjchem-1701	204	2	:	:	PUNCT
eurjchem-1701	204	3	yellow	yellow	ADJ
eurjchem-1701	204	4	.	.	PUNCT
eurjchem-1701	205	1	yield	yield	NOUN
eurjchem-1701	205	2	:	:	PUNCT
eurjchem-1701	205	3	70	70	NUM
eurjchem-1701	205	4	%	%	NOUN
eurjchem-1701	205	5	.	.	PUNCT
eurjchem-1701	206	1	m.p	m.p	PROPN
eurjchem-1701	206	2	.	.	PROPN
eurjchem-1701	206	3	:	:	PUNCT
eurjchem-1701	207	1	236	236	NUM
eurjchem-1701	207	2	-	-	SYM
eurjchem-1701	207	3	237	237	NUM
eurjchem-1701	207	4	°	°	NOUN
eurjchem-1701	207	5	c	c	NOUN
eurjchem-1701	207	6	.	.	PUNCT
eurjchem-1701	208	1	ft	ft	PROPN
eurjchem-1701	208	2	-	-	PUNCT
eurjchem-1701	208	3	ir	ir	PROPN
eurjchem-1701	208	4	(	(	PUNCT
eurjchem-1701	208	5	kbr	kbr	PROPN
eurjchem-1701	208	6	,	,	PUNCT
eurjchem-1701	208	7	ν	ν	PROPN
eurjchem-1701	208	8	,	,	PUNCT
eurjchem-1701	208	9	cm-1	cm-1	NUM
eurjchem-1701	208	10	):	):	PUNCT
eurjchem-1701	208	11	3412	3412	NUM
eurjchem-1701	208	12	,	,	PUNCT
eurjchem-1701	208	13	3261(2nh	3261(2nh	NUM
eurjchem-1701	208	14	)	)	PUNCT
eurjchem-1701	208	15	,	,	PUNCT
eurjchem-1701	208	16	1735	1735	NUM
eurjchem-1701	208	17	(	(	PUNCT
eurjchem-1701	208	18	c	c	NOUN
eurjchem-1701	208	19	=	=	NOUN
eurjchem-1701	208	20	o	o	NOUN
eurjchem-1701	208	21	)	)	PUNCT
eurjchem-1701	208	22	(	(	PUNCT
eurjchem-1701	208	23	ester	ester	NOUN
eurjchem-1701	208	24	)	)	PUNCT
eurjchem-1701	208	25	,	,	PUNCT
eurjchem-1701	208	26	1677	1677	NUM
eurjchem-1701	208	27	(	(	PUNCT
eurjchem-1701	208	28	c	c	NOUN
eurjchem-1701	208	29	=	=	NOUN
eurjchem-1701	208	30	o	o	NOUN
eurjchem-1701	208	31	)	)	PUNCT
eurjchem-1701	208	32	(	(	PUNCT
eurjchem-1701	208	33	amide	amide	NOUN
eurjchem-1701	208	34	)	)	PUNCT
eurjchem-1701	208	35	,	,	PUNCT
eurjchem-1701	208	36	1649	1649	NUM
eurjchem-1701	208	37	(	(	PUNCT
eurjchem-1701	208	38	c	c	NOUN
eurjchem-1701	208	39	=	=	SYM
eurjchem-1701	208	40	c	c	NOUN
eurjchem-1701	208	41	)	)	PUNCT
eurjchem-1701	208	42	.	.	PUNCT
eurjchem-1701	209	1	1h	1h	NUM
eurjchem-1701	209	2	nmr	nmr	NOUN
eurjchem-1701	209	3	(	(	PUNCT
eurjchem-1701	209	4	300	300	NUM
eurjchem-1701	209	5	mhz	mhz	NOUN
eurjchem-1701	209	6	,	,	PUNCT
eurjchem-1701	209	7	dmso	dmso	NOUN
eurjchem-1701	209	8	-	-	NOUN
eurjchem-1701	209	9	d6	d6	NOUN
eurjchem-1701	209	10	,	,	PUNCT
eurjchem-1701	209	11	δ	δ	PROPN
eurjchem-1701	209	12	,	,	PUNCT
eurjchem-1701	209	13	ppm	ppm	NUM
eurjchem-1701	209	14	):	):	PUNCT
eurjchem-1701	209	15	1.34	1.34	NUM
eurjchem-1701	209	16	(	(	PUNCT
eurjchem-1701	209	17	t	t	PROPN
eurjchem-1701	209	18	,	,	PUNCT
eurjchem-1701	209	19	j	j	PROPN
eurjchem-1701	209	20	=	=	PROPN
eurjchem-1701	209	21	2.3	2.3	NUM
eurjchem-1701	209	22	hz	hz	NOUN
eurjchem-1701	209	23	,	,	PUNCT
eurjchem-1701	209	24	3h	3h	NUM
eurjchem-1701	209	25	,	,	PUNCT
eurjchem-1701	209	26	ch3	ch3	PROPN
eurjchem-1701	209	27	)	)	PUNCT
eurjchem-1701	209	28	,	,	PUNCT
eurjchem-1701	209	29	1.72	1.72	NUM
eurjchem-1701	209	30	(	(	PUNCT
eurjchem-1701	209	31	m	m	PROPN
eurjchem-1701	209	32	,	,	PUNCT
eurjchem-1701	209	33	4h	4h	NOUN
eurjchem-1701	209	34	,	,	PUNCT
eurjchem-1701	209	35	cyclohexane2ch2	cyclohexane2ch2	NOUN
eurjchem-1701	209	36	)	)	PUNCT
eurjchem-1701	209	37	,	,	PUNCT
eurjchem-1701	209	38	2.63	2.63	NUM
eurjchem-1701	209	39	(	(	PUNCT
eurjchem-1701	209	40	t	t	PROPN
eurjchem-1701	209	41	,	,	PUNCT
eurjchem-1701	209	42	j	j	PROPN
eurjchem-1701	209	43	=	=	SYM
eurjchem-1701	209	44	5.6	5.6	NUM
eurjchem-1701	209	45	hz	hz	NOUN
eurjchem-1701	209	46	,	,	PUNCT
eurjchem-1701	209	47	2h	2h	NUM
eurjchem-1701	209	48	,	,	PUNCT
eurjchem-1701	209	49	cyclohexane	cyclohexane	NOUN
eurjchem-1701	209	50	-	-	PUNCT
eurjchem-1701	209	51	ch2	ch2	NOUN
eurjchem-1701	209	52	)	)	PUNCT
eurjchem-1701	209	53	,	,	PUNCT
eurjchem-1701	209	54	2.75	2.75	NUM
eurjchem-1701	209	55	(	(	PUNCT
eurjchem-1701	209	56	t	t	PROPN
eurjchem-1701	209	57	,	,	PUNCT
eurjchem-1701	209	58	j	j	PROPN
eurjchem-1701	209	59	=	=	SYM
eurjchem-1701	209	60	5.6	5.6	NUM
eurjchem-1701	209	61	hz	hz	NOUN
eurjchem-1701	209	62	,	,	PUNCT
eurjchem-1701	209	63	2h	2h	NUM
eurjchem-1701	209	64	,	,	PUNCT
eurjchem-1701	209	65	cyclohexane	cyclohexane	NOUN
eurjchem-1701	209	66	-	-	PUNCT
eurjchem-1701	209	67	ch2	ch2	NOUN
eurjchem-1701	209	68	)	)	PUNCT
eurjchem-1701	209	69	,	,	PUNCT
eurjchem-1701	209	70	4.37	4.37	NUM
eurjchem-1701	209	71	(	(	PUNCT
eurjchem-1701	209	72	q	q	NOUN
eurjchem-1701	209	73	,	,	PUNCT
eurjchem-1701	209	74	j	j	PROPN
eurjchem-1701	209	75	=	=	SYM
eurjchem-1701	209	76	2.3	2.3	NUM
eurjchem-1701	209	77	hz	hz	NOUN
eurjchem-1701	209	78	,	,	PUNCT
eurjchem-1701	209	79	2h	2h	NUM
eurjchem-1701	209	80	,	,	PUNCT
eurjchem-1701	209	81	ch2	ch2	PROPN
eurjchem-1701	209	82	)	)	PUNCT
eurjchem-1701	209	83	,	,	PUNCT
eurjchem-1701	209	84	7.24	7.24	NUM
eurjchem-1701	209	85	(	(	PUNCT
eurjchem-1701	209	86	d	d	PROPN
eurjchem-1701	209	87	,	,	PUNCT
eurjchem-1701	209	88	j	j	PROPN
eurjchem-1701	209	89	=	=	SYM
eurjchem-1701	209	90	3.6	3.6	NUM
eurjchem-1701	209	91	hz	hz	NOUN
eurjchem-1701	209	92	,	,	PUNCT
eurjchem-1701	209	93	1h	1h	NUM
eurjchem-1701	209	94	,	,	PUNCT
eurjchem-1701	209	95	thiophene	thiophene	NOUN
eurjchem-1701	209	96	-	-	PUNCT
eurjchem-1701	209	97	hc	hc	NOUN
eurjchem-1701	209	98	)	)	PUNCT
eurjchem-1701	209	99	,	,	PUNCT
eurjchem-1701	209	100	8.06	8.06	NUM
eurjchem-1701	209	101	(	(	PUNCT
eurjchem-1701	209	102	d	d	PROPN
eurjchem-1701	209	103	,	,	PUNCT
eurjchem-1701	209	104	j	j	PROPN
eurjchem-1701	209	105	=	=	SYM
eurjchem-1701	209	106	4.8	4.8	NUM
eurjchem-1701	209	107	hz	hz	NOUN
eurjchem-1701	209	108	,	,	PUNCT
eurjchem-1701	209	109	1h	1h	NUM
eurjchem-1701	209	110	,	,	PUNCT
eurjchem-1701	209	111	thiopheneha	thiopheneha	NOUN
eurjchem-1701	209	112	)	)	PUNCT
eurjchem-1701	209	113	,	,	PUNCT
eurjchem-1701	209	114	8.38	8.38	NUM
eurjchem-1701	209	115	(	(	PUNCT
eurjchem-1701	209	116	t	t	PROPN
eurjchem-1701	209	117	,	,	PUNCT
eurjchem-1701	209	118	j	j	PROPN
eurjchem-1701	209	119	=	=	SYM
eurjchem-1701	209	120	4.8	4.8	NUM
eurjchem-1701	209	121	hz	hz	VERB
eurjchem-1701	209	122	,	,	PUNCT
eurjchem-1701	209	123	j	j	PROPN
eurjchem-1701	210	1	=	=	SYM
eurjchem-1701	210	2	3.6	3.6	NUM
eurjchem-1701	210	3	hz	hz	NOUN
eurjchem-1701	210	4	,	,	PUNCT
eurjchem-1701	210	5	1h	1h	NUM
eurjchem-1701	210	6	,	,	PUNCT
eurjchem-1701	210	7	thiophene	thiophene	NOUN
eurjchem-1701	210	8	-	-	PUNCT
eurjchem-1701	210	9	hb	hb	NOUN
eurjchem-1701	210	10	)	)	PUNCT
eurjchem-1701	210	11	,	,	PUNCT
eurjchem-1701	210	12	11.84	11.84	NUM
eurjchem-1701	210	13	(	(	PUNCT
eurjchem-1701	210	14	s	s	PROPN
eurjchem-1701	210	15	,	,	PUNCT
eurjchem-1701	210	16	1h	1h	NUM
eurjchem-1701	210	17	,	,	PUNCT
eurjchem-1701	210	18	d2o	d2o	NOUN
eurjchem-1701	210	19	exchangeable	exchangeable	ADJ
eurjchem-1701	210	20	,	,	PUNCT
eurjchem-1701	210	21	nh	nh	PROPN
eurjchem-1701	210	22	)	)	PUNCT
eurjchem-1701	210	23	,	,	PUNCT
eurjchem-1701	210	24	14.61	14.61	NUM
eurjchem-1701	210	25	(	(	PUNCT
eurjchem-1701	210	26	s	s	PROPN
eurjchem-1701	210	27	,	,	PUNCT
eurjchem-1701	210	28	1h	1h	NUM
eurjchem-1701	210	29	,	,	PUNCT
eurjchem-1701	210	30	d2o	d2o	NOUN
eurjchem-1701	210	31	exchangeable	exchangeable	ADJ
eurjchem-1701	210	32	,	,	PUNCT
eurjchem-1701	210	33	nh	nh	PROPN
eurjchem-1701	210	34	)	)	PUNCT
eurjchem-1701	210	35	.	.	PUNCT
eurjchem-1701	211	1	13c	13c	NOUN
eurjchem-1701	211	2	nmr	nmr	NOUN
eurjchem-1701	211	3	(	(	PUNCT
eurjchem-1701	211	4	75.4	75.4	NUM
eurjchem-1701	211	5	mhz	mhz	NOUN
eurjchem-1701	211	6	,	,	PUNCT
eurjchem-1701	211	7	dmso	dmso	NOUN
eurjchem-1701	211	8	-	-	NOUN
eurjchem-1701	211	9	d6	d6	NOUN
eurjchem-1701	211	10	,	,	PUNCT
eurjchem-1701	211	11	δ	δ	PROPN
eurjchem-1701	211	12	,	,	PUNCT
eurjchem-1701	211	13	ppm	ppm	NOUN
eurjchem-1701	211	14	):	):	PUNCT
eurjchem-1701	211	15	167.3	167.3	NUM
eurjchem-1701	211	16	(	(	PUNCT
eurjchem-1701	211	17	1c	1c	NOUN
eurjchem-1701	211	18	,	,	PUNCT
eurjchem-1701	211	19	c	c	PROPN
eurjchem-1701	211	20	=	=	SYM
eurjchem-1701	211	21	s	s	NOUN
eurjchem-1701	211	22	)	)	PUNCT
eurjchem-1701	211	23	,	,	PUNCT
eurjchem-1701	211	24	162.4	162.4	NUM
eurjchem-1701	211	25	,	,	PUNCT
eurjchem-1701	211	26	161.7	161.7	NUM
eurjchem-1701	211	27	(	(	PUNCT
eurjchem-1701	211	28	2c	2c	NOUN
eurjchem-1701	211	29	,	,	PUNCT
eurjchem-1701	211	30	2c	2c	NOUN
eurjchem-1701	211	31	=	=	SYM
eurjchem-1701	211	32	o	o	NOUN
eurjchem-1701	211	33	)	)	PUNCT
eurjchem-1701	211	34	,	,	PUNCT
eurjchem-1701	211	35	150.1	150.1	NUM
eurjchem-1701	211	36	,	,	PUNCT
eurjchem-1701	211	37	132.6	132.6	NUM
eurjchem-1701	211	38	,	,	PUNCT
eurjchem-1701	211	39	130.8	130.8	NUM
eurjchem-1701	211	40	,	,	PUNCT
eurjchem-1701	211	41	129.2	129.2	NUM
eurjchem-1701	211	42	,	,	PUNCT
eurjchem-1701	211	43	128.4	128.4	NUM
eurjchem-1701	211	44	,	,	PUNCT
eurjchem-1701	211	45	126.2	126.2	NUM
eurjchem-1701	211	46	,	,	PUNCT
eurjchem-1701	211	47	125.4	125.4	NUM
eurjchem-1701	211	48	,	,	PUNCT
eurjchem-1701	211	49	114.2	114.2	NUM
eurjchem-1701	211	50	(	(	PUNCT
eurjchem-1701	211	51	ar	ar	NOUN
eurjchem-1701	211	52	-	-	NOUN
eurjchem-1701	211	53	c	c	NOUN
eurjchem-1701	211	54	)	)	PUNCT
eurjchem-1701	211	55	,	,	PUNCT
eurjchem-1701	211	56	61.2	61.2	NUM
eurjchem-1701	211	57	(	(	PUNCT
eurjchem-1701	211	58	1c	1c	NOUN
eurjchem-1701	211	59	,	,	PUNCT
eurjchem-1701	211	60	och2	och2	PROPN
eurjchem-1701	211	61	)	)	PUNCT
eurjchem-1701	211	62	,	,	PUNCT
eurjchem-1701	211	63	25.8	25.8	NUM
eurjchem-1701	211	64	,	,	PUNCT
eurjchem-1701	211	65	23.9	23.9	NUM
eurjchem-1701	211	66	,	,	PUNCT
eurjchem-1701	211	67	23.2	23.2	NUM
eurjchem-1701	211	68	,	,	PUNCT
eurjchem-1701	211	69	22.5	22.5	NUM
eurjchem-1701	211	70	(	(	PUNCT
eurjchem-1701	211	71	4c	4c	NOUN
eurjchem-1701	211	72	,	,	PUNCT
eurjchem-1701	211	73	4ch2	4ch2	NUM
eurjchem-1701	211	74	-	-	PUNCT
eurjchem-1701	211	75	cyclohexane	cyclohexane	NOUN
eurjchem-1701	211	76	)	)	PUNCT
eurjchem-1701	211	77	,	,	PUNCT
eurjchem-1701	211	78	14.3	14.3	NUM
eurjchem-1701	211	79	(	(	PUNCT
eurjchem-1701	211	80	1c	1c	NOUN
eurjchem-1701	211	81	,	,	PUNCT
eurjchem-1701	211	82	ch3	ch3	PROPN
eurjchem-1701	211	83	)	)	PUNCT
eurjchem-1701	211	84	.	.	PUNCT
eurjchem-1701	212	1	ms	ms	PROPN
eurjchem-1701	212	2	(	(	PUNCT
eurjchem-1701	212	3	ei	ei	PROPN
eurjchem-1701	212	4	,	,	PUNCT
eurjchem-1701	212	5	m	m	PROPN
eurjchem-1701	212	6	/	/	SYM
eurjchem-1701	212	7	z	z	PROPN
eurjchem-1701	212	8	(	(	PUNCT
eurjchem-1701	212	9	%	%	NOUN
eurjchem-1701	212	10	)	)	PUNCT
eurjchem-1701	212	11	):	):	PUNCT
eurjchem-1701	212	12	394	394	NUM
eurjchem-1701	212	13	(	(	PUNCT
eurjchem-1701	212	14	m+	m+	NUM
eurjchem-1701	212	15	,	,	PUNCT
eurjchem-1701	212	16	100	100	NUM
eurjchem-1701	212	17	)	)	PUNCT
eurjchem-1701	212	18	,	,	PUNCT
eurjchem-1701	212	19	267	267	NUM
eurjchem-1701	212	20	(	(	PUNCT
eurjchem-1701	212	21	10	10	NUM
eurjchem-1701	212	22	)	)	PUNCT
eurjchem-1701	212	23	,	,	PUNCT
eurjchem-1701	212	24	225	225	NUM
eurjchem-1701	212	25	(	(	PUNCT
eurjchem-1701	212	26	40	40	NUM
eurjchem-1701	212	27	)	)	PUNCT
eurjchem-1701	212	28	,	,	PUNCT
eurjchem-1701	212	29	179	179	NUM
eurjchem-1701	212	30	(	(	PUNCT
eurjchem-1701	212	31	65	65	NUM
eurjchem-1701	212	32	)	)	PUNCT
eurjchem-1701	212	33	,	,	PUNCT
eurjchem-1701	212	34	150	150	NUM
eurjchem-1701	212	35	(	(	PUNCT
eurjchem-1701	212	36	30	30	NUM
eurjchem-1701	212	37	)	)	PUNCT
eurjchem-1701	212	38	,	,	PUNCT
eurjchem-1701	212	39	110	110	NUM
eurjchem-1701	212	40	(	(	PUNCT
eurjchem-1701	212	41	25	25	NUM
eurjchem-1701	212	42	)	)	PUNCT
eurjchem-1701	212	43	.	.	PUNCT
eurjchem-1701	213	1	anal	anal	PROPN
eurjchem-1701	213	2	.	.	PUNCT
eurjchem-1701	213	3	calcd	calcd	NOUN
eurjchem-1701	213	4	.	.	PUNCT
eurjchem-1701	214	1	for	for	ADP
eurjchem-1701	214	2	c17h18n2o3s3	c17h18n2o3s3	PROPN
eurjchem-1701	214	3	:	:	PUNCT
eurjchem-1701	214	4	c	c	X
eurjchem-1701	214	5	,	,	PUNCT
eurjchem-1701	214	6	51.75	51.75	NUM
eurjchem-1701	214	7	;	;	PUNCT
eurjchem-1701	214	8	h	h	NOUN
eurjchem-1701	214	9	,	,	PUNCT
eurjchem-1701	214	10	4.60	4.60	NUM
eurjchem-1701	214	11	;	;	PUNCT
eurjchem-1701	214	12	n	n	CCONJ
eurjchem-1701	214	13	,	,	PUNCT
eurjchem-1701	214	14	7.10	7.10	NUM
eurjchem-1701	214	15	.	.	PUNCT
eurjchem-1701	214	16	found	find	VERB
eurjchem-1701	214	17	:	:	PUNCT
eurjchem-1701	215	1	c	c	X
eurjchem-1701	215	2	,	,	PUNCT
eurjchem-1701	215	3	51.66	51.66	NUM
eurjchem-1701	215	4	;	;	PUNCT
eurjchem-1701	215	5	h	h	NOUN
eurjchem-1701	215	6	,	,	PUNCT
eurjchem-1701	215	7	4.52	4.52	NUM
eurjchem-1701	215	8	;	;	PUNCT
eurjchem-1701	215	9	n	n	CCONJ
eurjchem-1701	215	10	,	,	PUNCT
eurjchem-1701	215	11	7.02	7.02	NUM
eurjchem-1701	215	12	%	%	NOUN
eurjchem-1701	215	13	.	.	PUNCT
eurjchem-1701	216	1	2.3.13	2.3.13	NUM
eurjchem-1701	216	2	.	.	PUNCT
eurjchem-1701	217	1	synthesis	synthesis	NOUN
eurjchem-1701	217	2	of	of	ADP
eurjchem-1701	217	3	2-(3-(thiophene-2	2-(3-(thiophene-2	NUM
eurjchem-1701	217	4	-	-	PUNCT
eurjchem-1701	217	5	carbonyl)thiourei	carbonyl)thiourei	ADJ
eurjchem-1701	217	6	do)-4,5,6,7	do)-4,5,6,7	NOUN
eurjchem-1701	217	7	-	-	PUNCT
eurjchem-1701	217	8	tetrahydrobenzo[b]thiophene-3	tetrahydrobenzo[b]thiophene-3	NOUN
eurjchem-1701	217	9	-	-	PUNCT
eurjchem-1701	217	10	carboxylic	carboxylic	ADJ
eurjchem-1701	217	11	acid	acid	NOUN
eurjchem-1701	217	12	(	(	PUNCT
eurjchem-1701	217	13	16	16	NUM
eurjchem-1701	217	14	)	)	PUNCT
eurjchem-1701	217	15	a	a	DET
eurjchem-1701	217	16	mixture	mixture	NOUN
eurjchem-1701	217	17	of	of	ADP
eurjchem-1701	217	18	ethyl	ethyl	PROPN
eurjchem-1701	217	19	2-(3-(thiophene-2	2-(3-(thiophene-2	NUM
eurjchem-1701	217	20	-	-	PUNCT
eurjchem-1701	217	21	carbonyl)thioureido)-4	carbonyl)thioureido)-4	VERB
eurjchem-1701	217	22	,	,	PUNCT
eurjchem-1701	217	23	5	5	NUM
eurjchem-1701	217	24	,	,	PUNCT
eurjchem-1701	217	25	6	6	NUM
eurjchem-1701	217	26	,	,	PUNCT
eurjchem-1701	217	27	7	7	NUM
eurjchem-1701	217	28	-	-	PUNCT
eurjchem-1701	217	29	tetrahydrobenzo[b]thiophene-3	tetrahydrobenzo[b]thiophene-3	NOUN
eurjchem-1701	217	30	-	-	PUNCT
eurjchem-1701	217	31	carboxylate	carboxylate	NOUN
eurjchem-1701	217	32	(	(	PUNCT
eurjchem-1701	217	33	15	15	NUM
eurjchem-1701	217	34	)	)	PUNCT
eurjchem-1701	217	35	(	(	PUNCT
eurjchem-1701	217	36	1.26	1.26	NUM
eurjchem-1701	217	37	mol	mol	NOUN
eurjchem-1701	217	38	)	)	PUNCT
eurjchem-1701	217	39	and	and	CCONJ
eurjchem-1701	217	40	sodium	sodium	NOUN
eurjchem-1701	217	41	ethoxide	ethoxide	NOUN
eurjchem-1701	217	42	(	(	PUNCT
eurjchem-1701	217	43	1.26	1.26	NUM
eurjchem-1701	217	44	mol	mol	NOUN
eurjchem-1701	217	45	)	)	PUNCT
eurjchem-1701	217	46	in	in	ADP
eurjchem-1701	217	47	ethanol	ethanol	NOUN
eurjchem-1701	217	48	(	(	PUNCT
eurjchem-1701	217	49	20	20	NUM
eurjchem-1701	217	50	ml	ml	NOUN
eurjchem-1701	217	51	)	)	PUNCT
eurjchem-1701	217	52	was	be	AUX
eurjchem-1701	217	53	heated	heat	VERB
eurjchem-1701	217	54	under	under	ADP
eurjchem-1701	217	55	reflux	reflux	NOUN
eurjchem-1701	217	56	for	for	ADP
eurjchem-1701	217	57	6	6	NUM
eurjchem-1701	217	58	h.	h.	NOUN
eurjchem-1701	217	59	the	the	DET
eurjchem-1701	217	60	reaction	reaction	NOUN
eurjchem-1701	217	61	mixture	mixture	NOUN
eurjchem-1701	217	62	was	be	AUX
eurjchem-1701	217	63	neutralized	neutralize	VERB
eurjchem-1701	217	64	by	by	ADP
eurjchem-1701	217	65	10	10	NUM
eurjchem-1701	217	66	%	%	NOUN
eurjchem-1701	217	67	hcl	hcl	PROPN
eurjchem-1701	217	68	.	.	PUNCT
eurjchem-1701	218	1	the	the	DET
eurjchem-1701	218	2	formed	form	VERB
eurjchem-1701	218	3	precipitate	precipitate	NOUN
eurjchem-1701	218	4	was	be	AUX
eurjchem-1701	218	5	filtered	filter	VERB
eurjchem-1701	218	6	off	off	ADP
eurjchem-1701	218	7	,	,	PUNCT
eurjchem-1701	218	8	dried	dry	VERB
eurjchem-1701	218	9	and	and	CCONJ
eurjchem-1701	218	10	crystallized	crystallize	VERB
eurjchem-1701	218	11	from	from	ADP
eurjchem-1701	218	12	ethanol	ethanol	NOUN
eurjchem-1701	218	13	to	to	PART
eurjchem-1701	218	14	give	give	VERB
eurjchem-1701	218	15	compound	compound	NOUN
eurjchem-1701	218	16	16	16	NUM
eurjchem-1701	218	17	(	(	PUNCT
eurjchem-1701	218	18	scheme	scheme	NOUN
eurjchem-1701	218	19	5	5	NUM
eurjchem-1701	218	20	)	)	PUNCT
eurjchem-1701	218	21	.	.	PUNCT
eurjchem-1701	219	1	color	color	NOUN
eurjchem-1701	219	2	:	:	PUNCT
eurjchem-1701	219	3	yellow	yellow	ADJ
eurjchem-1701	219	4	.	.	PUNCT
eurjchem-1701	220	1	yield	yield	NOUN
eurjchem-1701	220	2	:	:	PUNCT
eurjchem-1701	220	3	86	86	NUM
eurjchem-1701	220	4	%	%	NOUN
eurjchem-1701	220	5	.	.	PUNCT
eurjchem-1701	221	1	m.p	m.p	PROPN
eurjchem-1701	221	2	.	.	PROPN
eurjchem-1701	221	3	:	:	PUNCT
eurjchem-1701	222	1	282	282	NUM
eurjchem-1701	222	2	-	-	SYM
eurjchem-1701	222	3	283	283	NUM
eurjchem-1701	222	4	°	°	NOUN
eurjchem-1701	222	5	c	c	NOUN
eurjchem-1701	222	6	.	.	PUNCT
eurjchem-1701	222	7	ft	ft	PROPN
eurjchem-1701	222	8	-	-	PUNCT
eurjchem-1701	222	9	ir	ir	PROPN
eurjchem-1701	222	10	(	(	PUNCT
eurjchem-1701	222	11	kbr	kbr	PROPN
eurjchem-1701	222	12	,	,	PUNCT
eurjchem-1701	222	13	ν	ν	PROPN
eurjchem-1701	222	14	,	,	PUNCT
eurjchem-1701	222	15	cm-1	cm-1	NUM
eurjchem-1701	222	16	):	):	PUNCT
eurjchem-1701	222	17	3654	3654	NUM
eurjchem-1701	222	18	(	(	PUNCT
eurjchem-1701	222	19	oh	oh	INTJ
eurjchem-1701	222	20	)	)	PUNCT
eurjchem-1701	222	21	,	,	PUNCT
eurjchem-1701	222	22	3424	3424	NUM
eurjchem-1701	222	23	(	(	PUNCT
eurjchem-1701	222	24	nh	nh	NOUN
eurjchem-1701	222	25	)	)	PUNCT
eurjchem-1701	222	26	,	,	PUNCT
eurjchem-1701	222	27	1697	1697	NUM
eurjchem-1701	222	28	(	(	PUNCT
eurjchem-1701	222	29	c	c	NOUN
eurjchem-1701	222	30	=	=	NOUN
eurjchem-1701	222	31	o	o	NOUN
eurjchem-1701	222	32	)	)	PUNCT
eurjchem-1701	222	33	(	(	PUNCT
eurjchem-1701	222	34	acid	acid	NOUN
eurjchem-1701	222	35	)	)	PUNCT
eurjchem-1701	222	36	,	,	PUNCT
eurjchem-1701	222	37	1676	1676	NUM
eurjchem-1701	222	38	(	(	PUNCT
eurjchem-1701	222	39	c	c	NOUN
eurjchem-1701	222	40	=	=	NOUN
eurjchem-1701	222	41	o	o	NOUN
eurjchem-1701	222	42	)	)	PUNCT
eurjchem-1701	222	43	(	(	PUNCT
eurjchem-1701	222	44	amide	amide	NOUN
eurjchem-1701	222	45	)	)	PUNCT
eurjchem-1701	222	46	.	.	PUNCT
eurjchem-1701	223	1	2018	2018	NUM
eurjchem-1701	223	2	–	–	PUNCT
eurjchem-1701	223	3	european	european	ADJ
eurjchem-1701	223	4	journal	journal	NOUN
eurjchem-1701	223	5	of	of	ADP
eurjchem-1701	223	6	chemistry	chemistry	NOUN
eurjchem-1701	223	7	–	–	PUNCT
eurjchem-1701	223	8	cc	cc	NOUN
eurjchem-1701	223	9	by	by	ADP
eurjchem-1701	223	10	nc	nc	PROPN
eurjchem-1701	223	11	–	–	PUNCT
eurjchem-1701	223	12	doi	doi	NOUN
eurjchem-1701	223	13	:	:	PUNCT
eurjchem-1701	223	14	10.5155	10.5155	NUM
eurjchem-1701	223	15	/	/	SYM
eurjchem-1701	223	16	eurjchem.9.2.99	eurjchem.9.2.99	NUM
eurjchem-1701	223	17	-	-	PUNCT
eurjchem-1701	223	18	106.1701	106.1701	NUM
eurjchem-1701	223	19	104	104	NUM
eurjchem-1701	223	20	haggam	haggam	NOUN
eurjchem-1701	223	21	et	et	PROPN
eurjchem-1701	223	22	al	al	PROPN
eurjchem-1701	223	23	.	.	PUNCT
eurjchem-1701	223	24	/	/	SYM
eurjchem-1701	223	25	european	european	PROPN
eurjchem-1701	223	26	journal	journal	PROPN
eurjchem-1701	223	27	of	of	ADP
eurjchem-1701	223	28	chemistry	chemistry	NOUN
eurjchem-1701	223	29	9	9	NUM
eurjchem-1701	223	30	(	(	PUNCT
eurjchem-1701	223	31	2	2	NUM
eurjchem-1701	223	32	)	)	PUNCT
eurjchem-1701	223	33	(	(	PUNCT
eurjchem-1701	223	34	2018	2018	NUM
eurjchem-1701	223	35	)	)	PUNCT
eurjchem-1701	223	36	99	99	NUM
eurjchem-1701	223	37	-	-	SYM
eurjchem-1701	223	38	106	106	NUM
eurjchem-1701	223	39	dioxane	dioxane	NOUN
eurjchem-1701	223	40	reflux	reflux	NOUN
eurjchem-1701	223	41	1	1	NUM
eurjchem-1701	223	42	h	h	NOUN
eurjchem-1701	223	43	86	86	NUM
eurjchem-1701	223	44	%	%	NOUN
eurjchem-1701	223	45	70	70	NUM
eurjchem-1701	223	46	%	%	NOUN
eurjchem-1701	223	47	s	s	PART
eurjchem-1701	223	48	nh2	nh2	NOUN
eurjchem-1701	223	49	cooet	cooet	NOUN
eurjchem-1701	223	50	s	s	PART
eurjchem-1701	223	51	n	n	NUM
eurjchem-1701	223	52	h	h	NOUN
eurjchem-1701	224	1	n	n	NOUN
eurjchem-1701	224	2	h	h	NOUN
eurjchem-1701	224	3	s	s	PART
eurjchem-1701	224	4	o	o	NOUN
eurjchem-1701	224	5	s	s	X
eurjchem-1701	224	6	s	s	X
eurjchem-1701	224	7	n	n	PRON
eurjchem-1701	224	8	h	h	NOUN
eurjchem-1701	224	9	cooh	cooh	NOUN
eurjchem-1701	225	1	n	n	PRON
eurjchem-1701	225	2	h	h	NOUN
eurjchem-1701	225	3	s	s	PART
eurjchem-1701	225	4	o	o	NOUN
eurjchem-1701	225	5	s	s	X
eurjchem-1701	225	6	s	s	X
eurjchem-1701	225	7	n	n	NUM
eurjchem-1701	225	8	h	h	NOUN
eurjchem-1701	226	1	n	n	NOUN
eurjchem-1701	226	2	s	s	NOUN
eurjchem-1701	226	3	o	o	NOUN
eurjchem-1701	226	4	o	o	X
eurjchem-1701	226	5	s	s	VERB
eurjchem-1701	226	6	cooet	cooet	NOUN
eurjchem-1701	227	1	hn	hn	PROPN
eurjchem-1701	228	1	n	n	ADV
eurjchem-1701	228	2	h	h	NOUN
eurjchem-1701	228	3	s	s	PART
eurjchem-1701	228	4	o	o	NOUN
eurjchem-1701	228	5	s	s	VERB
eurjchem-1701	228	6	hn	hn	NOUN
eurjchem-1701	228	7	h	h	NOUN
eurjchem-1701	228	8	n	n	NOUN
eurjchem-1701	228	9	s	s	PROPN
eurjchem-1701	228	10	o	o	NOUN
eurjchem-1701	228	11	s	s	NOUN
eurjchem-1701	229	1	n	n	NUM
eurjchem-1701	229	2	h	h	NOUN
eurjchem-1701	230	1	o	o	X
eurjchem-1701	230	2	sn	sn	PROPN
eurjchem-1701	230	3	n	n	PROPN
eurjchem-1701	230	4	s	s	PROPN
eurjchem-1701	230	5	nh	nh	NOUN
eurjchem-1701	230	6	o	o	NOUN
eurjchem-1701	230	7	s	s	PROPN
eurjchem-1701	230	8	h2s	h2s	NOUN
eurjchem-1701	230	9	nh2	nh2	PROPN
eurjchem-1701	230	10	nh2	nh2	PROPN
eurjchem-1701	230	11	15	15	NUM
eurjchem-1701	230	12	16	16	NUM
eurjchem-1701	230	13	17	17	NUM
eurjchem-1701	230	14	19	19	NUM
eurjchem-1701	230	15	so3h	so3h	NUM
eurjchem-1701	230	16	nh2	nh2	NOUN
eurjchem-1701	230	17	oh	oh	NUM
eurjchem-1701	230	18	so3h	so3h	NUM
eurjchem-1701	230	19	nh2	nh2	PROPN
eurjchem-1701	230	20	o	o	NOUN
eurjchem-1701	230	21	n	n	CCONJ
eurjchem-1701	230	22	s	s	NOUN
eurjchem-1701	230	23	s	s	PROPN
eurjchem-1701	230	24	18	18	NUM
eurjchem-1701	230	25	1	1	NUM
eurjchem-1701	230	26	s	s	NOUN
eurjchem-1701	230	27	o	o	NOUN
eurjchem-1701	230	28	n	n	ADP
eurjchem-1701	230	29	c	c	NOUN
eurjchem-1701	230	30	s	s	PROPN
eurjchem-1701	230	31	etona	etona	PROPN
eurjchem-1701	230	32	reflux	reflux	VERB
eurjchem-1701	230	33	6	6	NUM
eurjchem-1701	230	34	h	h	NOUN
eurjchem-1701	230	35	dioxane	dioxane	NOUN
eurjchem-1701	230	36	reflux	reflux	NOUN
eurjchem-1701	230	37	2	2	NUM
eurjchem-1701	230	38	h	h	NOUN
eurjchem-1701	230	39	65	65	NUM
eurjchem-1701	230	40	%	%	NOUN
eurjchem-1701	230	41	dioxane	dioxane	NOUN
eurjchem-1701	230	42	reflux	reflux	NOUN
eurjchem-1701	230	43	2	2	NUM
eurjchem-1701	230	44	h	h	NOUN
eurjchem-1701	230	45	74	74	NUM
eurjchem-1701	230	46	%	%	NOUN
eurjchem-1701	230	47	scheme	scheme	NOUN
eurjchem-1701	230	48	5	5	NUM
eurjchem-1701	230	49	1h	1h	NUM
eurjchem-1701	230	50	nmr	nmr	NOUN
eurjchem-1701	230	51	(	(	PUNCT
eurjchem-1701	230	52	300	300	NUM
eurjchem-1701	230	53	mhz	mhz	NOUN
eurjchem-1701	230	54	,	,	PUNCT
eurjchem-1701	230	55	dmso	dmso	NOUN
eurjchem-1701	230	56	-	-	NOUN
eurjchem-1701	230	57	d6	d6	NOUN
eurjchem-1701	230	58	,	,	PUNCT
eurjchem-1701	230	59	δ	δ	PROPN
eurjchem-1701	230	60	,	,	PUNCT
eurjchem-1701	230	61	ppm	ppm	NUM
eurjchem-1701	230	62	):	):	PUNCT
eurjchem-1701	230	63	1.75	1.75	NUM
eurjchem-1701	230	64	(	(	PUNCT
eurjchem-1701	230	65	m	m	PROPN
eurjchem-1701	230	66	,	,	PUNCT
eurjchem-1701	230	67	4h	4h	NOUN
eurjchem-1701	230	68	,	,	PUNCT
eurjchem-1701	230	69	cyclohexane-2ch2	cyclohexane-2ch2	PROPN
eurjchem-1701	230	70	)	)	PUNCT
eurjchem-1701	230	71	,	,	PUNCT
eurjchem-1701	230	72	2.67	2.67	NUM
eurjchem-1701	230	73	(	(	PUNCT
eurjchem-1701	230	74	t	t	PROPN
eurjchem-1701	230	75	,	,	PUNCT
eurjchem-1701	230	76	j	j	PROPN
eurjchem-1701	230	77	=	=	SYM
eurjchem-1701	230	78	5.6	5.6	NUM
eurjchem-1701	230	79	hz	hz	NOUN
eurjchem-1701	230	80	,	,	PUNCT
eurjchem-1701	230	81	2h	2h	NUM
eurjchem-1701	230	82	,	,	PUNCT
eurjchem-1701	230	83	cyclohexane	cyclohexane	NOUN
eurjchem-1701	230	84	-	-	PUNCT
eurjchem-1701	230	85	ch2	ch2	NOUN
eurjchem-1701	230	86	)	)	PUNCT
eurjchem-1701	230	87	,	,	PUNCT
eurjchem-1701	230	88	2.71	2.71	NUM
eurjchem-1701	230	89	(	(	PUNCT
eurjchem-1701	230	90	t	t	PROPN
eurjchem-1701	230	91	,	,	PUNCT
eurjchem-1701	230	92	j	j	PROPN
eurjchem-1701	231	1	=	=	SYM
eurjchem-1701	231	2	5.6	5.6	NUM
eurjchem-1701	231	3	hz	hz	NOUN
eurjchem-1701	231	4	,	,	PUNCT
eurjchem-1701	231	5	2h	2h	NUM
eurjchem-1701	231	6	,	,	PUNCT
eurjchem-1701	231	7	cyclohexane	cyclohexane	NOUN
eurjchem-1701	231	8	-	-	PUNCT
eurjchem-1701	231	9	ch2	ch2	NOUN
eurjchem-1701	231	10	)	)	PUNCT
eurjchem-1701	231	11	,	,	PUNCT
eurjchem-1701	231	12	7.23	7.23	NUM
eurjchem-1701	231	13	(	(	PUNCT
eurjchem-1701	231	14	d	d	PROPN
eurjchem-1701	231	15	,	,	PUNCT
eurjchem-1701	231	16	j	j	PROPN
eurjchem-1701	231	17	=	=	SYM
eurjchem-1701	231	18	3.6	3.6	NUM
eurjchem-1701	231	19	hz	hz	NOUN
eurjchem-1701	231	20	,	,	PUNCT
eurjchem-1701	231	21	1h	1h	NUM
eurjchem-1701	231	22	,	,	PUNCT
eurjchem-1701	231	23	thiophene	thiophene	NOUN
eurjchem-1701	231	24	-	-	PUNCT
eurjchem-1701	231	25	hc	hc	NOUN
eurjchem-1701	231	26	)	)	PUNCT
eurjchem-1701	231	27	,	,	PUNCT
eurjchem-1701	231	28	8.01	8.01	NUM
eurjchem-1701	231	29	(	(	PUNCT
eurjchem-1701	231	30	d	d	PROPN
eurjchem-1701	231	31	,	,	PUNCT
eurjchem-1701	231	32	j	j	PROPN
eurjchem-1701	231	33	=	=	SYM
eurjchem-1701	231	34	4.8	4.8	NUM
eurjchem-1701	231	35	hz	hz	NOUN
eurjchem-1701	231	36	,	,	PUNCT
eurjchem-1701	231	37	1h	1h	NUM
eurjchem-1701	231	38	,	,	PUNCT
eurjchem-1701	231	39	thiophene	thiophene	NOUN
eurjchem-1701	231	40	-	-	PUNCT
eurjchem-1701	231	41	ha	ha	NOUN
eurjchem-1701	231	42	)	)	PUNCT
eurjchem-1701	231	43	,	,	PUNCT
eurjchem-1701	231	44	8.29	8.29	NUM
eurjchem-1701	231	45	(	(	PUNCT
eurjchem-1701	231	46	t	t	PROPN
eurjchem-1701	231	47	,	,	PUNCT
eurjchem-1701	231	48	j	j	PROPN
eurjchem-1701	231	49	=	=	SYM
eurjchem-1701	231	50	4.8	4.8	NUM
eurjchem-1701	231	51	hz	hz	VERB
eurjchem-1701	231	52	,	,	PUNCT
eurjchem-1701	231	53	j	j	PROPN
eurjchem-1701	232	1	=	=	SYM
eurjchem-1701	232	2	3.6	3.6	NUM
eurjchem-1701	232	3	hz	hz	NOUN
eurjchem-1701	232	4	,	,	PUNCT
eurjchem-1701	232	5	1h	1h	NUM
eurjchem-1701	232	6	,	,	PUNCT
eurjchem-1701	232	7	thiophene	thiophene	NOUN
eurjchem-1701	232	8	-	-	PUNCT
eurjchem-1701	232	9	hb	hb	NOUN
eurjchem-1701	232	10	)	)	PUNCT
eurjchem-1701	232	11	,	,	PUNCT
eurjchem-1701	232	12	11.76	11.76	NUM
eurjchem-1701	232	13	(	(	PUNCT
eurjchem-1701	232	14	s	s	PROPN
eurjchem-1701	232	15	,	,	PUNCT
eurjchem-1701	232	16	1h	1h	NUM
eurjchem-1701	232	17	,	,	PUNCT
eurjchem-1701	232	18	d2o	d2o	NOUN
eurjchem-1701	232	19	exchangeable	exchangeable	ADJ
eurjchem-1701	232	20	,	,	PUNCT
eurjchem-1701	232	21	nh	nh	PROPN
eurjchem-1701	232	22	)	)	PUNCT
eurjchem-1701	232	23	,	,	PUNCT
eurjchem-1701	232	24	13.29	13.29	NUM
eurjchem-1701	232	25	(	(	PUNCT
eurjchem-1701	232	26	s	s	PROPN
eurjchem-1701	232	27	,	,	PUNCT
eurjchem-1701	232	28	1h	1h	NUM
eurjchem-1701	232	29	,	,	PUNCT
eurjchem-1701	232	30	d2o	d2o	NOUN
eurjchem-1701	232	31	exchangeable	exchangeable	ADJ
eurjchem-1701	232	32	,	,	PUNCT
eurjchem-1701	232	33	nh	nh	PROPN
eurjchem-1701	232	34	)	)	PUNCT
eurjchem-1701	232	35	,	,	PUNCT
eurjchem-1701	232	36	14.61	14.61	NUM
eurjchem-1701	232	37	(	(	PUNCT
eurjchem-1701	232	38	s	s	PROPN
eurjchem-1701	232	39	,	,	PUNCT
eurjchem-1701	232	40	1h	1h	NUM
eurjchem-1701	232	41	,	,	PUNCT
eurjchem-1701	232	42	d2o	d2o	NOUN
eurjchem-1701	232	43	exchangeable	exchangeable	ADJ
eurjchem-1701	232	44	,	,	PUNCT
eurjchem-1701	232	45	oh	oh	INTJ
eurjchem-1701	232	46	)	)	PUNCT
eurjchem-1701	232	47	.	.	PUNCT
eurjchem-1701	233	1	13c	13c	NOUN
eurjchem-1701	233	2	nmr	nmr	NOUN
eurjchem-1701	233	3	(	(	PUNCT
eurjchem-1701	233	4	75.4	75.4	NUM
eurjchem-1701	233	5	mhz	mhz	NOUN
eurjchem-1701	233	6	,	,	PUNCT
eurjchem-1701	233	7	dmso	dmso	NOUN
eurjchem-1701	233	8	-	-	NOUN
eurjchem-1701	233	9	d6	d6	NOUN
eurjchem-1701	233	10	,	,	PUNCT
eurjchem-1701	233	11	δ	δ	PROPN
eurjchem-1701	233	12	,	,	PUNCT
eurjchem-1701	233	13	ppm	ppm	NUM
eurjchem-1701	233	14	):	):	PUNCT
eurjchem-1701	233	15	167.4	167.4	NUM
eurjchem-1701	233	16	(	(	PUNCT
eurjchem-1701	233	17	1c	1c	NOUN
eurjchem-1701	233	18	,	,	PUNCT
eurjchem-1701	233	19	c	c	PROPN
eurjchem-1701	233	20	=	=	SYM
eurjchem-1701	233	21	s	s	NOUN
eurjchem-1701	233	22	)	)	PUNCT
eurjchem-1701	233	23	,	,	PUNCT
eurjchem-1701	233	24	165.6	165.6	NUM
eurjchem-1701	233	25	,	,	PUNCT
eurjchem-1701	233	26	164.7	164.7	NUM
eurjchem-1701	233	27	(	(	PUNCT
eurjchem-1701	233	28	2c	2c	NOUN
eurjchem-1701	233	29	,	,	PUNCT
eurjchem-1701	233	30	2c	2c	NOUN
eurjchem-1701	233	31	=	=	SYM
eurjchem-1701	233	32	o	o	NOUN
eurjchem-1701	233	33	)	)	PUNCT
eurjchem-1701	233	34	,	,	PUNCT
eurjchem-1701	233	35	149.8	149.8	NUM
eurjchem-1701	233	36	,	,	PUNCT
eurjchem-1701	233	37	132.0	132.0	NUM
eurjchem-1701	233	38	,	,	PUNCT
eurjchem-1701	233	39	130.3	130.3	NUM
eurjchem-1701	233	40	,	,	PUNCT
eurjchem-1701	233	41	129.4	129.4	NUM
eurjchem-1701	233	42	,	,	PUNCT
eurjchem-1701	233	43	128.1	128.1	NUM
eurjchem-1701	233	44	,	,	PUNCT
eurjchem-1701	233	45	126.6	126.6	NUM
eurjchem-1701	233	46	,	,	PUNCT
eurjchem-1701	233	47	125.0	125.0	NUM
eurjchem-1701	233	48	,	,	PUNCT
eurjchem-1701	233	49	114.7	114.7	NUM
eurjchem-1701	233	50	(	(	PUNCT
eurjchem-1701	233	51	ar	ar	NOUN
eurjchem-1701	233	52	-	-	NOUN
eurjchem-1701	233	53	c	c	NOUN
eurjchem-1701	233	54	)	)	PUNCT
eurjchem-1701	233	55	,	,	PUNCT
eurjchem-1701	233	56	25.0	25.0	NUM
eurjchem-1701	233	57	,	,	PUNCT
eurjchem-1701	233	58	24.1	24.1	NUM
eurjchem-1701	233	59	,	,	PUNCT
eurjchem-1701	233	60	23.4	23.4	NUM
eurjchem-1701	233	61	,	,	PUNCT
eurjchem-1701	233	62	22.7	22.7	NUM
eurjchem-1701	233	63	(	(	PUNCT
eurjchem-1701	233	64	4c	4c	NOUN
eurjchem-1701	233	65	,	,	PUNCT
eurjchem-1701	233	66	4ch2	4ch2	NUM
eurjchem-1701	233	67	-	-	PUNCT
eurjchem-1701	233	68	cyclohexane	cyclohexane	NOUN
eurjchem-1701	233	69	)	)	PUNCT
eurjchem-1701	233	70	.	.	PUNCT
eurjchem-1701	234	1	ms	ms	NOUN
eurjchem-1701	234	2	(	(	PUNCT
eurjchem-1701	234	3	ei	ei	PROPN
eurjchem-1701	234	4	,	,	PUNCT
eurjchem-1701	234	5	m	m	PROPN
eurjchem-1701	234	6	/	/	SYM
eurjchem-1701	234	7	z	z	PROPN
eurjchem-1701	234	8	(	(	PUNCT
eurjchem-1701	234	9	%	%	NOUN
eurjchem-1701	234	10	)	)	PUNCT
eurjchem-1701	234	11	):	):	PUNCT
eurjchem-1701	234	12	366	366	NUM
eurjchem-1701	234	13	(	(	PUNCT
eurjchem-1701	234	14	m+	m+	NUM
eurjchem-1701	234	15	,	,	PUNCT
eurjchem-1701	234	16	100	100	NUM
eurjchem-1701	234	17	)	)	PUNCT
eurjchem-1701	234	18	,	,	PUNCT
eurjchem-1701	234	19	287(20	287(20	NUM
eurjchem-1701	234	20	)	)	PUNCT
eurjchem-1701	234	21	,	,	PUNCT
eurjchem-1701	234	22	237(95	237(95	NUM
eurjchem-1701	234	23	)	)	PUNCT
eurjchem-1701	234	24	,	,	PUNCT
eurjchem-1701	234	25	178(45	178(45	NUM
eurjchem-1701	234	26	)	)	PUNCT
eurjchem-1701	234	27	,	,	PUNCT
eurjchem-1701	234	28	150(40	150(40	NUM
eurjchem-1701	234	29	)	)	PUNCT
eurjchem-1701	234	30	,	,	PUNCT
eurjchem-1701	234	31	110(10	110(10	NUM
eurjchem-1701	234	32	)	)	PUNCT
eurjchem-1701	234	33	.	.	PUNCT
eurjchem-1701	235	1	anal	anal	PROPN
eurjchem-1701	235	2	.	.	PUNCT
eurjchem-1701	235	3	calcd	calcd	NOUN
eurjchem-1701	235	4	.	.	PUNCT
eurjchem-1701	236	1	for	for	ADP
eurjchem-1701	236	2	c15h14n2o3s3	c15h14n2o3s3	NOUN
eurjchem-1701	236	3	:	:	PUNCT
eurjchem-1701	236	4	c	c	X
eurjchem-1701	236	5	,	,	PUNCT
eurjchem-1701	236	6	49.16	49.16	NUM
eurjchem-1701	236	7	;	;	PUNCT
eurjchem-1701	236	8	h	h	NOUN
eurjchem-1701	236	9	,	,	PUNCT
eurjchem-1701	236	10	3.85	3.85	NUM
eurjchem-1701	236	11	;	;	PUNCT
eurjchem-1701	236	12	n	n	CCONJ
eurjchem-1701	236	13	,	,	PUNCT
eurjchem-1701	236	14	7.64	7.64	NUM
eurjchem-1701	236	15	.	.	PUNCT
eurjchem-1701	236	16	found	find	VERB
eurjchem-1701	236	17	:	:	PUNCT
eurjchem-1701	237	1	c	c	X
eurjchem-1701	237	2	,	,	PUNCT
eurjchem-1701	237	3	49.09	49.09	NUM
eurjchem-1701	237	4	;	;	PUNCT
eurjchem-1701	237	5	h	h	NOUN
eurjchem-1701	237	6	,	,	PUNCT
eurjchem-1701	237	7	3.72	3.72	NUM
eurjchem-1701	237	8	;	;	PUNCT
eurjchem-1701	237	9	n	n	CCONJ
eurjchem-1701	237	10	,	,	PUNCT
eurjchem-1701	237	11	7.54	7.54	NUM
eurjchem-1701	237	12	%	%	NOUN
eurjchem-1701	237	13	.	.	PUNCT
eurjchem-1701	238	1	2.3.14	2.3.14	NUM
eurjchem-1701	238	2	.	.	PUNCT
eurjchem-1701	239	1	synthesis	synthesis	NOUN
eurjchem-1701	239	2	of	of	ADP
eurjchem-1701	239	3	10	10	NUM
eurjchem-1701	239	4	-	-	PUNCT
eurjchem-1701	239	5	amino-2-(thiophen-2	amino-2-(thiophen-2	NOUN
eurjchem-1701	239	6	-	-	PUNCT
eurjchem-1701	239	7	yl)-4	yl)-4	VERB
eurjchem-1701	239	8	-	-	PUNCT
eurjchem-1701	239	9	thioxo4h	thioxo4h	NOUN
eurjchem-1701	239	10	-	-	PUNCT
eurjchem-1701	239	11	naphtho[2,3	naphtho[2,3	NUM
eurjchem-1701	239	12	-	-	PUNCT
eurjchem-1701	239	13	e][1,3]oxazine-5	e][1,3]oxazine-5	ADJ
eurjchem-1701	239	14	-	-	PUNCT
eurjchem-1701	239	15	sulfonic	sulfonic	ADJ
eurjchem-1701	239	16	acid	acid	NOUN
eurjchem-1701	239	17	(	(	PUNCT
eurjchem-1701	239	18	18	18	NUM
eurjchem-1701	239	19	)	)	PUNCT
eurjchem-1701	239	20	a	a	DET
eurjchem-1701	239	21	mixture	mixture	NOUN
eurjchem-1701	239	22	of	of	ADP
eurjchem-1701	239	23	thiophene-2	thiophene-2	NOUN
eurjchem-1701	239	24	-	-	PUNCT
eurjchem-1701	239	25	carbonylisothiocyanate	carbonylisothiocyanate	NOUN
eurjchem-1701	239	26	(	(	PUNCT
eurjchem-1701	239	27	1	1	NUM
eurjchem-1701	239	28	)	)	PUNCT
eurjchem-1701	239	29	(	(	PUNCT
eurjchem-1701	239	30	3.34	3.34	NUM
eurjchem-1701	239	31	mol	mol	NOUN
eurjchem-1701	239	32	)	)	PUNCT
eurjchem-1701	239	33	and	and	CCONJ
eurjchem-1701	239	34	4	4	NUM
eurjchem-1701	239	35	-	-	PUNCT
eurjchem-1701	239	36	amino-3	amino-3	NUM
eurjchem-1701	239	37	-	-	PUNCT
eurjchem-1701	239	38	hydroxynaphthalene-1	hydroxynaphthalene-1	NOUN
eurjchem-1701	239	39	-	-	PUNCT
eurjchem-1701	239	40	sulfonic	sulfonic	ADJ
eurjchem-1701	239	41	acid	acid	NOUN
eurjchem-1701	239	42	(	(	PUNCT
eurjchem-1701	239	43	3.34	3.34	NUM
eurjchem-1701	239	44	mmol	mmol	NOUN
eurjchem-1701	239	45	)	)	PUNCT
eurjchem-1701	239	46	in	in	ADP
eurjchem-1701	239	47	dioxane	dioxane	NOUN
eurjchem-1701	239	48	(	(	PUNCT
eurjchem-1701	239	49	20	20	NUM
eurjchem-1701	239	50	ml	ml	NOUN
eurjchem-1701	239	51	)	)	PUNCT
eurjchem-1701	239	52	was	be	AUX
eurjchem-1701	239	53	heated	heat	VERB
eurjchem-1701	239	54	under	under	ADP
eurjchem-1701	239	55	reflux	reflux	NOUN
eurjchem-1701	239	56	for	for	ADP
eurjchem-1701	239	57	2	2	NUM
eurjchem-1701	239	58	h.	h.	NOUN
eurjchem-1701	239	59	the	the	DET
eurjchem-1701	239	60	reaction	reaction	NOUN
eurjchem-1701	239	61	mixture	mixture	NOUN
eurjchem-1701	239	62	was	be	AUX
eurjchem-1701	239	63	poured	pour	VERB
eurjchem-1701	239	64	into	into	ADP
eurjchem-1701	239	65	water	water	NOUN
eurjchem-1701	239	66	.	.	PUNCT
eurjchem-1701	240	1	the	the	DET
eurjchem-1701	240	2	formed	form	VERB
eurjchem-1701	240	3	precipitate	precipitate	NOUN
eurjchem-1701	240	4	was	be	AUX
eurjchem-1701	240	5	filtered	filter	VERB
eurjchem-1701	240	6	off	off	ADP
eurjchem-1701	240	7	,	,	PUNCT
eurjchem-1701	240	8	washed	wash	VERB
eurjchem-1701	240	9	with	with	ADP
eurjchem-1701	240	10	water	water	NOUN
eurjchem-1701	240	11	,	,	PUNCT
eurjchem-1701	240	12	dried	dry	VERB
eurjchem-1701	240	13	and	and	CCONJ
eurjchem-1701	240	14	crystallized	crystallize	VERB
eurjchem-1701	240	15	from	from	ADP
eurjchem-1701	240	16	ethanol	ethanol	NOUN
eurjchem-1701	240	17	to	to	PART
eurjchem-1701	240	18	give	give	VERB
eurjchem-1701	240	19	compound	compound	NOUN
eurjchem-1701	240	20	18	18	NUM
eurjchem-1701	240	21	(	(	PUNCT
eurjchem-1701	240	22	scheme	scheme	NOUN
eurjchem-1701	240	23	5	5	NUM
eurjchem-1701	240	24	)	)	PUNCT
eurjchem-1701	240	25	.	.	PUNCT
eurjchem-1701	241	1	color	color	NOUN
eurjchem-1701	241	2	:	:	PUNCT
eurjchem-1701	241	3	brown	brown	ADJ
eurjchem-1701	241	4	.	.	PUNCT
eurjchem-1701	242	1	yield	yield	NOUN
eurjchem-1701	242	2	:	:	PUNCT
eurjchem-1701	242	3	65	65	NUM
eurjchem-1701	242	4	%	%	NOUN
eurjchem-1701	242	5	.	.	PUNCT
eurjchem-1701	243	1	m.p	m.p	PROPN
eurjchem-1701	243	2	.	.	PROPN
eurjchem-1701	243	3	:	:	PUNCT
eurjchem-1701	244	1	322	322	NUM
eurjchem-1701	244	2	-	-	SYM
eurjchem-1701	244	3	323	323	NUM
eurjchem-1701	244	4	°	°	NOUN
eurjchem-1701	244	5	c	c	NOUN
eurjchem-1701	244	6	.	.	PUNCT
eurjchem-1701	245	1	ft	ft	PROPN
eurjchem-1701	245	2	-	-	PUNCT
eurjchem-1701	245	3	ir	ir	PROPN
eurjchem-1701	245	4	(	(	PUNCT
eurjchem-1701	245	5	kbr	kbr	PROPN
eurjchem-1701	245	6	,	,	PUNCT
eurjchem-1701	245	7	ν	ν	PROPN
eurjchem-1701	245	8	,	,	PUNCT
eurjchem-1701	245	9	cm1	cm1	PROPN
eurjchem-1701	245	10	):	):	PUNCT
eurjchem-1701	245	11	3652	3652	NUM
eurjchem-1701	245	12	(	(	PUNCT
eurjchem-1701	245	13	oh	oh	INTJ
eurjchem-1701	245	14	)	)	PUNCT
eurjchem-1701	245	15	,	,	PUNCT
eurjchem-1701	245	16	3237	3237	NUM
eurjchem-1701	245	17	(	(	PUNCT
eurjchem-1701	245	18	nh2	nh2	PROPN
eurjchem-1701	245	19	)	)	PUNCT
eurjchem-1701	245	20	,	,	PUNCT
eurjchem-1701	245	21	1352(c	1352(c	PROPN
eurjchem-1701	245	22	-	-	PUNCT
eurjchem-1701	245	23	o	o	NOUN
eurjchem-1701	245	24	)	)	PUNCT
eurjchem-1701	245	25	.	.	PUNCT
eurjchem-1701	246	1	1h	1h	NUM
eurjchem-1701	246	2	nmr	nmr	NOUN
eurjchem-1701	246	3	(	(	PUNCT
eurjchem-1701	246	4	300	300	NUM
eurjchem-1701	246	5	mhz	mhz	NOUN
eurjchem-1701	246	6	,	,	PUNCT
eurjchem-1701	246	7	dmso	dmso	NOUN
eurjchem-1701	246	8	-	-	NOUN
eurjchem-1701	246	9	d6	d6	NOUN
eurjchem-1701	246	10	,	,	PUNCT
eurjchem-1701	246	11	δ	δ	PROPN
eurjchem-1701	246	12	,	,	PUNCT
eurjchem-1701	246	13	ppm	ppm	NUM
eurjchem-1701	246	14	):	):	PUNCT
eurjchem-1701	246	15	8.80	8.80	NUM
eurjchem-1701	246	16	-	-	SYM
eurjchem-1701	246	17	7.38	7.38	NUM
eurjchem-1701	246	18	(	(	PUNCT
eurjchem-1701	246	19	m	m	PROPN
eurjchem-1701	246	20	,	,	PUNCT
eurjchem-1701	246	21	7h	7h	PROPN
eurjchem-1701	246	22	,	,	PUNCT
eurjchem-1701	246	23	arh	arh	PROPN
eurjchem-1701	246	24	’s	’s	PART
eurjchem-1701	246	25	+	+	NUM
eurjchem-1701	246	26	thiophene	thiophene	NOUN
eurjchem-1701	246	27	protons	proton	NOUN
eurjchem-1701	246	28	)	)	PUNCT
eurjchem-1701	246	29	,	,	PUNCT
eurjchem-1701	246	30	9.78	9.78	NUM
eurjchem-1701	246	31	-	-	SYM
eurjchem-1701	246	32	9.74	9.74	NUM
eurjchem-1701	246	33	(	(	PUNCT
eurjchem-1701	246	34	br	br	NOUN
eurjchem-1701	246	35	s	s	PROPN
eurjchem-1701	246	36	,	,	PUNCT
eurjchem-1701	246	37	2h	2h	NUM
eurjchem-1701	246	38	,	,	PUNCT
eurjchem-1701	246	39	d2o	d2o	NOUN
eurjchem-1701	246	40	exchangeable	exchangeable	ADJ
eurjchem-1701	246	41	,	,	PUNCT
eurjchem-1701	246	42	nh2	nh2	PROPN
eurjchem-1701	246	43	)	)	PUNCT
eurjchem-1701	246	44	,	,	PUNCT
eurjchem-1701	246	45	11.00	11.00	NUM
eurjchem-1701	246	46	(	(	PUNCT
eurjchem-1701	246	47	s	s	PROPN
eurjchem-1701	246	48	,	,	PUNCT
eurjchem-1701	246	49	1h	1h	NUM
eurjchem-1701	246	50	,	,	PUNCT
eurjchem-1701	246	51	d2o	d2o	NOUN
eurjchem-1701	246	52	exchangeable	exchangeable	ADJ
eurjchem-1701	246	53	,	,	PUNCT
eurjchem-1701	246	54	oh	oh	INTJ
eurjchem-1701	246	55	)	)	PUNCT
eurjchem-1701	246	56	.	.	PUNCT
eurjchem-1701	247	1	ms	ms	NOUN
eurjchem-1701	247	2	(	(	PUNCT
eurjchem-1701	247	3	ei	ei	PROPN
eurjchem-1701	247	4	,	,	PUNCT
eurjchem-1701	247	5	m	m	PROPN
eurjchem-1701	247	6	/	/	SYM
eurjchem-1701	247	7	z	z	PROPN
eurjchem-1701	247	8	(	(	PUNCT
eurjchem-1701	247	9	%	%	NOUN
eurjchem-1701	247	10	)	)	PUNCT
eurjchem-1701	247	11	):	):	PUNCT
eurjchem-1701	248	1	390(m+	390(m+	NUM
eurjchem-1701	248	2	,	,	PUNCT
eurjchem-1701	248	3	100	100	NUM
eurjchem-1701	248	4	)	)	PUNCT
eurjchem-1701	248	5	,	,	PUNCT
eurjchem-1701	248	6	280	280	NUM
eurjchem-1701	248	7	(	(	PUNCT
eurjchem-1701	248	8	70	70	NUM
eurjchem-1701	248	9	)	)	PUNCT
eurjchem-1701	248	10	,	,	PUNCT
eurjchem-1701	248	11	168	168	NUM
eurjchem-1701	248	12	(	(	PUNCT
eurjchem-1701	248	13	50	50	NUM
eurjchem-1701	248	14	)	)	PUNCT
eurjchem-1701	248	15	,	,	PUNCT
eurjchem-1701	248	16	159	159	NUM
eurjchem-1701	248	17	(	(	PUNCT
eurjchem-1701	248	18	90	90	NUM
eurjchem-1701	248	19	)	)	PUNCT
eurjchem-1701	248	20	,	,	PUNCT
eurjchem-1701	248	21	129	129	NUM
eurjchem-1701	248	22	(	(	PUNCT
eurjchem-1701	248	23	40	40	NUM
eurjchem-1701	248	24	)	)	PUNCT
eurjchem-1701	248	25	,	,	PUNCT
eurjchem-1701	248	26	112	112	NUM
eurjchem-1701	248	27	(	(	PUNCT
eurjchem-1701	248	28	20	20	NUM
eurjchem-1701	248	29	)	)	PUNCT
eurjchem-1701	248	30	.	.	PUNCT
eurjchem-1701	249	1	anal	anal	PROPN
eurjchem-1701	249	2	.	.	PUNCT
eurjchem-1701	249	3	calcd	calcd	NOUN
eurjchem-1701	249	4	.	.	PUNCT
eurjchem-1701	250	1	for	for	ADP
eurjchem-1701	250	2	c16h10n2o4s3	c16h10n2o4s3	NOUN
eurjchem-1701	250	3	:	:	PUNCT
eurjchem-1701	250	4	c	c	X
eurjchem-1701	250	5	,	,	PUNCT
eurjchem-1701	250	6	49.22	49.22	NUM
eurjchem-1701	250	7	;	;	PUNCT
eurjchem-1701	250	8	h	h	NOUN
eurjchem-1701	250	9	,	,	PUNCT
eurjchem-1701	250	10	2.58	2.58	NUM
eurjchem-1701	250	11	;	;	PUNCT
eurjchem-1701	250	12	n	n	CCONJ
eurjchem-1701	250	13	,	,	PUNCT
eurjchem-1701	250	14	7.17	7.17	NUM
eurjchem-1701	250	15	.	.	PUNCT
eurjchem-1701	250	16	found	find	VERB
eurjchem-1701	250	17	:	:	PUNCT
eurjchem-1701	251	1	c	c	X
eurjchem-1701	251	2	,	,	PUNCT
eurjchem-1701	251	3	49.11	49.11	NUM
eurjchem-1701	251	4	;	;	PUNCT
eurjchem-1701	251	5	h	h	NOUN
eurjchem-1701	251	6	,	,	PUNCT
eurjchem-1701	251	7	2.53	2.53	NUM
eurjchem-1701	251	8	;	;	PUNCT
eurjchem-1701	251	9	n	n	CCONJ
eurjchem-1701	251	10	,	,	PUNCT
eurjchem-1701	251	11	7.14	7.14	NUM
eurjchem-1701	251	12	%	%	NOUN
eurjchem-1701	251	13	.	.	PUNCT
eurjchem-1701	252	1	2.3.15	2.3.15	X
eurjchem-1701	252	2	.	.	PUNCT
eurjchem-1701	253	1	synthesis	synthesis	NOUN
eurjchem-1701	253	2	of	of	ADP
eurjchem-1701	253	3	n-(4,5	n-(4,5	NOUN
eurjchem-1701	253	4	-	-	PUNCT
eurjchem-1701	253	5	dihydro-1-(sulfanylene(thiophene-2	dihydro-1-(sulfanylene(thiophene-2	PROPN
eurjchem-1701	253	6	-	-	PUNCT
eurjchem-1701	253	7	carboxamido)methyl)-1h	carboxamido)methyl)-1h	ADJ
eurjchem-1701	253	8	-	-	PUNCT
eurjchem-1701	253	9	imidazol-2	imidazol-2	NUM
eurjchem-1701	253	10	-	-	PUNCT
eurjchem-1701	253	11	yl)thiophene-2carboxamide	yl)thiophene-2carboxamide	NOUN
eurjchem-1701	253	12	(	(	PUNCT
eurjchem-1701	253	13	19	19	NUM
eurjchem-1701	253	14	)	)	PUNCT
eurjchem-1701	253	15	a	a	DET
eurjchem-1701	253	16	mixture	mixture	NOUN
eurjchem-1701	253	17	of	of	ADP
eurjchem-1701	253	18	thiophene-2	thiophene-2	NOUN
eurjchem-1701	253	19	-	-	PUNCT
eurjchem-1701	253	20	carbonylisothiocyanate	carbonylisothiocyanate	NOUN
eurjchem-1701	253	21	(	(	PUNCT
eurjchem-1701	253	22	1	1	NUM
eurjchem-1701	253	23	)	)	PUNCT
eurjchem-1701	253	24	(	(	PUNCT
eurjchem-1701	253	25	3.34	3.34	NUM
eurjchem-1701	253	26	mol	mol	NOUN
eurjchem-1701	253	27	)	)	PUNCT
eurjchem-1701	253	28	and	and	CCONJ
eurjchem-1701	253	29	ethylene	ethylene	NOUN
eurjchem-1701	253	30	diamine	diamine	NOUN
eurjchem-1701	253	31	(	(	PUNCT
eurjchem-1701	253	32	3.34	3.34	NUM
eurjchem-1701	253	33	mol	mol	NOUN
eurjchem-1701	253	34	)	)	PUNCT
eurjchem-1701	253	35	in	in	ADP
eurjchem-1701	253	36	dioxane	dioxane	NOUN
eurjchem-1701	253	37	(	(	PUNCT
eurjchem-1701	253	38	20	20	NUM
eurjchem-1701	253	39	ml	ml	NOUN
eurjchem-1701	253	40	)	)	PUNCT
eurjchem-1701	253	41	was	be	AUX
eurjchem-1701	253	42	heated	heat	VERB
eurjchem-1701	253	43	under	under	ADP
eurjchem-1701	253	44	reflux	reflux	NOUN
eurjchem-1701	253	45	for	for	ADP
eurjchem-1701	253	46	2	2	NUM
eurjchem-1701	253	47	h.	h.	NOUN
eurjchem-1701	253	48	the	the	DET
eurjchem-1701	253	49	reaction	reaction	NOUN
eurjchem-1701	253	50	mixture	mixture	NOUN
eurjchem-1701	253	51	was	be	AUX
eurjchem-1701	253	52	poured	pour	VERB
eurjchem-1701	253	53	into	into	ADP
eurjchem-1701	253	54	water	water	NOUN
eurjchem-1701	253	55	.	.	PUNCT
eurjchem-1701	254	1	the	the	DET
eurjchem-1701	254	2	formed	form	VERB
eurjchem-1701	254	3	precipitate	precipitate	NOUN
eurjchem-1701	254	4	was	be	AUX
eurjchem-1701	254	5	filtered	filter	VERB
eurjchem-1701	254	6	off	off	ADP
eurjchem-1701	254	7	,	,	PUNCT
eurjchem-1701	254	8	washed	wash	VERB
eurjchem-1701	254	9	with	with	ADP
eurjchem-1701	254	10	water	water	NOUN
eurjchem-1701	254	11	,	,	PUNCT
eurjchem-1701	254	12	dried	dry	VERB
eurjchem-1701	254	13	and	and	CCONJ
eurjchem-1701	254	14	crystallized	crystallize	VERB
eurjchem-1701	254	15	from	from	ADP
eurjchem-1701	254	16	ethanol	ethanol	NOUN
eurjchem-1701	254	17	to	to	PART
eurjchem-1701	254	18	give	give	VERB
eurjchem-1701	254	19	compound	compound	NOUN
eurjchem-1701	254	20	19	19	NUM
eurjchem-1701	254	21	(	(	PUNCT
eurjchem-1701	254	22	scheme	scheme	NOUN
eurjchem-1701	254	23	5	5	NUM
eurjchem-1701	254	24	)	)	PUNCT
eurjchem-1701	254	25	.	.	PUNCT
eurjchem-1701	255	1	color	color	NOUN
eurjchem-1701	255	2	:	:	PUNCT
eurjchem-1701	255	3	white	white	ADJ
eurjchem-1701	255	4	.	.	PUNCT
eurjchem-1701	256	1	yield	yield	NOUN
eurjchem-1701	256	2	:	:	PUNCT
eurjchem-1701	256	3	74	74	NUM
eurjchem-1701	256	4	%	%	NOUN
eurjchem-1701	256	5	.	.	PUNCT
eurjchem-1701	257	1	m.p	m.p	PROPN
eurjchem-1701	257	2	.	.	PROPN
eurjchem-1701	257	3	:	:	PUNCT
eurjchem-1701	258	1	328329	328329	NUM
eurjchem-1701	258	2	°	°	ADP
eurjchem-1701	258	3	c	c	NOUN
eurjchem-1701	258	4	.	.	PUNCT
eurjchem-1701	258	5	ft	ft	PROPN
eurjchem-1701	258	6	-	-	PUNCT
eurjchem-1701	258	7	ir	ir	PROPN
eurjchem-1701	258	8	(	(	PUNCT
eurjchem-1701	258	9	kbr	kbr	PROPN
eurjchem-1701	258	10	,	,	PUNCT
eurjchem-1701	258	11	ν	ν	PROPN
eurjchem-1701	258	12	,	,	PUNCT
eurjchem-1701	258	13	cm-1	cm-1	NUM
eurjchem-1701	258	14	):	):	PUNCT
eurjchem-1701	258	15	3391	3391	NUM
eurjchem-1701	258	16	,	,	PUNCT
eurjchem-1701	258	17	3290	3290	NUM
eurjchem-1701	258	18	(	(	PUNCT
eurjchem-1701	258	19	nh	nh	NOUN
eurjchem-1701	258	20	)	)	PUNCT
eurjchem-1701	258	21	,	,	PUNCT
eurjchem-1701	258	22	1674	1674	NUM
eurjchem-1701	258	23	,	,	PUNCT
eurjchem-1701	258	24	1665	1665	NUM
eurjchem-1701	258	25	(	(	PUNCT
eurjchem-1701	258	26	2c	2c	NOUN
eurjchem-1701	258	27	=	=	SYM
eurjchem-1701	258	28	o	o	NOUN
eurjchem-1701	258	29	)	)	PUNCT
eurjchem-1701	258	30	(	(	PUNCT
eurjchem-1701	258	31	amide	amide	NOUN
eurjchem-1701	258	32	)	)	PUNCT
eurjchem-1701	258	33	,	,	PUNCT
eurjchem-1701	258	34	1537	1537	NUM
eurjchem-1701	258	35	(	(	PUNCT
eurjchem-1701	258	36	c	c	NOUN
eurjchem-1701	258	37	=	=	SYM
eurjchem-1701	258	38	n	n	NUM
eurjchem-1701	258	39	)	)	PUNCT
eurjchem-1701	258	40	.	.	PUNCT
eurjchem-1701	259	1	1h	1h	NUM
eurjchem-1701	259	2	nmr	nmr	NOUN
eurjchem-1701	259	3	(	(	PUNCT
eurjchem-1701	259	4	300	300	NUM
eurjchem-1701	259	5	mhz	mhz	NOUN
eurjchem-1701	259	6	,	,	PUNCT
eurjchem-1701	259	7	dmso	dmso	NOUN
eurjchem-1701	259	8	-	-	NOUN
eurjchem-1701	259	9	d6	d6	NOUN
eurjchem-1701	259	10	,	,	PUNCT
eurjchem-1701	259	11	δ	δ	PROPN
eurjchem-1701	259	12	,	,	PUNCT
eurjchem-1701	259	13	ppm	ppm	NUM
eurjchem-1701	259	14	):	):	PUNCT
eurjchem-1701	259	15	3.33	3.33	NUM
eurjchem-1701	259	16	(	(	PUNCT
eurjchem-1701	259	17	t	t	PROPN
eurjchem-1701	259	18	,	,	PUNCT
eurjchem-1701	259	19	j	j	PROPN
eurjchem-1701	259	20	=	=	SYM
eurjchem-1701	259	21	2.6	2.6	NUM
eurjchem-1701	259	22	hz	hz	NOUN
eurjchem-1701	259	23	,	,	PUNCT
eurjchem-1701	259	24	2h	2h	NUM
eurjchem-1701	259	25	,	,	PUNCT
eurjchem-1701	259	26	ch2	ch2	PROPN
eurjchem-1701	259	27	)	)	PUNCT
eurjchem-1701	259	28	,	,	PUNCT
eurjchem-1701	259	29	3.94	3.94	NUM
eurjchem-1701	259	30	(	(	PUNCT
eurjchem-1701	259	31	t	t	PROPN
eurjchem-1701	259	32	,	,	PUNCT
eurjchem-1701	259	33	j	j	PROPN
eurjchem-1701	259	34	=	=	SYM
eurjchem-1701	259	35	2.6	2.6	NUM
eurjchem-1701	259	36	hz	hz	NOUN
eurjchem-1701	259	37	,	,	PUNCT
eurjchem-1701	259	38	2h	2h	NUM
eurjchem-1701	259	39	,	,	PUNCT
eurjchem-1701	259	40	ch2	ch2	PROPN
eurjchem-1701	259	41	)	)	PUNCT
eurjchem-1701	259	42	,	,	PUNCT
eurjchem-1701	259	43	8.65	8.65	NUM
eurjchem-1701	259	44	-	-	SYM
eurjchem-1701	259	45	7.13	7.13	NUM
eurjchem-1701	259	46	(	(	PUNCT
eurjchem-1701	259	47	m	m	PROPN
eurjchem-1701	259	48	,	,	PUNCT
eurjchem-1701	259	49	6h	6h	NUM
eurjchem-1701	259	50	,	,	PUNCT
eurjchem-1701	259	51	thiophene	thiophene	NOUN
eurjchem-1701	259	52	protons	proton	NOUN
eurjchem-1701	259	53	)	)	PUNCT
eurjchem-1701	259	54	,	,	PUNCT
eurjchem-1701	259	55	10.80	10.80	NUM
eurjchem-1701	259	56	(	(	PUNCT
eurjchem-1701	259	57	s	s	PROPN
eurjchem-1701	259	58	,	,	PUNCT
eurjchem-1701	259	59	1h	1h	NUM
eurjchem-1701	259	60	,	,	PUNCT
eurjchem-1701	259	61	d2o	d2o	NOUN
eurjchem-1701	259	62	exchangeable	exchangeable	ADJ
eurjchem-1701	259	63	,	,	PUNCT
eurjchem-1701	259	64	nh	nh	PROPN
eurjchem-1701	259	65	)	)	PUNCT
eurjchem-1701	259	66	,	,	PUNCT
eurjchem-1701	259	67	11.40	11.40	NUM
eurjchem-1701	259	68	(	(	PUNCT
eurjchem-1701	259	69	s	s	PROPN
eurjchem-1701	259	70	,	,	PUNCT
eurjchem-1701	259	71	1h	1h	NUM
eurjchem-1701	259	72	,	,	PUNCT
eurjchem-1701	259	73	d2o	d2o	NOUN
eurjchem-1701	259	74	exchangeable	exchangeable	ADJ
eurjchem-1701	259	75	,	,	PUNCT
eurjchem-1701	259	76	nh	nh	PROPN
eurjchem-1701	259	77	)	)	PUNCT
eurjchem-1701	259	78	.	.	PUNCT
eurjchem-1701	260	1	13c	13c	NOUN
eurjchem-1701	260	2	nmr	nmr	NOUN
eurjchem-1701	260	3	(	(	PUNCT
eurjchem-1701	260	4	75.4	75.4	NUM
eurjchem-1701	260	5	mhz	mhz	NOUN
eurjchem-1701	260	6	,	,	PUNCT
eurjchem-1701	260	7	dmso	dmso	NOUN
eurjchem-1701	260	8	-	-	NOUN
eurjchem-1701	260	9	d6	d6	NOUN
eurjchem-1701	260	10	,	,	PUNCT
eurjchem-1701	260	11	δ	δ	PROPN
eurjchem-1701	260	12	,	,	PUNCT
eurjchem-1701	260	13	ppm	ppm	NOUN
eurjchem-1701	260	14	):	):	PUNCT
eurjchem-1701	260	15	168.41	168.41	NUM
eurjchem-1701	260	16	(	(	PUNCT
eurjchem-1701	260	17	1c	1c	NOUN
eurjchem-1701	260	18	,	,	PUNCT
eurjchem-1701	260	19	c	c	PROPN
eurjchem-1701	260	20	=	=	SYM
eurjchem-1701	260	21	s	s	NOUN
eurjchem-1701	260	22	)	)	PUNCT
eurjchem-1701	260	23	,	,	PUNCT
eurjchem-1701	260	24	161.4	161.4	NUM
eurjchem-1701	260	25	(	(	PUNCT
eurjchem-1701	260	26	2c	2c	NOUN
eurjchem-1701	260	27	,	,	PUNCT
eurjchem-1701	260	28	2c	2c	NOUN
eurjchem-1701	260	29	=	=	SYM
eurjchem-1701	260	30	o	o	NOUN
eurjchem-1701	260	31	)	)	PUNCT
eurjchem-1701	260	32	,	,	PUNCT
eurjchem-1701	260	33	153.8	153.8	NUM
eurjchem-1701	260	34	(	(	PUNCT
eurjchem-1701	260	35	1c	1c	X
eurjchem-1701	260	36	,	,	PUNCT
eurjchem-1701	260	37	ncn	ncn	NOUN
eurjchem-1701	260	38	)	)	PUNCT
eurjchem-1701	260	39	,	,	PUNCT
eurjchem-1701	260	40	130.8	130.8	NUM
eurjchem-1701	260	41	,	,	PUNCT
eurjchem-1701	260	42	129.0	129.0	NUM
eurjchem-1701	260	43	,	,	PUNCT
eurjchem-1701	260	44	128.3	128.3	NUM
eurjchem-1701	260	45	,	,	PUNCT
eurjchem-1701	260	46	119.7	119.7	NUM
eurjchem-1701	260	47	(	(	PUNCT
eurjchem-1701	260	48	2arc	2arc	NUM
eurjchem-1701	260	49	)	)	PUNCT
eurjchem-1701	260	50	,	,	PUNCT
eurjchem-1701	260	51	54.4	54.4	NUM
eurjchem-1701	260	52	,	,	PUNCT
eurjchem-1701	260	53	52.7	52.7	NUM
eurjchem-1701	260	54	(	(	PUNCT
eurjchem-1701	260	55	1c	1c	NOUN
eurjchem-1701	260	56	,	,	PUNCT
eurjchem-1701	260	57	2ch2	2ch2	NUM
eurjchem-1701	260	58	-	-	PUNCT
eurjchem-1701	260	59	imidazole	imidazole	NOUN
eurjchem-1701	260	60	)	)	PUNCT
eurjchem-1701	260	61	.	.	PUNCT
eurjchem-1701	261	1	ms	ms	NOUN
eurjchem-1701	261	2	(	(	PUNCT
eurjchem-1701	261	3	ei	ei	PROPN
eurjchem-1701	261	4	,	,	PUNCT
eurjchem-1701	261	5	m	m	PROPN
eurjchem-1701	261	6	/	/	SYM
eurjchem-1701	261	7	z	z	PROPN
eurjchem-1701	261	8	(	(	PUNCT
eurjchem-1701	261	9	%	%	NOUN
eurjchem-1701	261	10	)	)	PUNCT
eurjchem-1701	261	11	):	):	PUNCT
eurjchem-1701	261	12	366	366	NUM
eurjchem-1701	261	13	(	(	PUNCT
eurjchem-1701	261	14	m+	m+	NUM
eurjchem-1701	261	15	,	,	PUNCT
eurjchem-1701	261	16	100	100	NUM
eurjchem-1701	261	17	)	)	PUNCT
eurjchem-1701	261	18	,	,	PUNCT
eurjchem-1701	261	19	364(m+	364(m+	PROPN
eurjchem-1701	261	20	,	,	PUNCT
eurjchem-1701	261	21	15	15	NUM
eurjchem-1701	261	22	)	)	PUNCT
eurjchem-1701	261	23	,	,	PUNCT
eurjchem-1701	261	24	261(10	261(10	NUM
eurjchem-1701	261	25	)	)	PUNCT
eurjchem-1701	261	26	,	,	PUNCT
eurjchem-1701	261	27	185(5	185(5	NUM
eurjchem-1701	261	28	)	)	PUNCT
eurjchem-1701	261	29	,	,	PUNCT
eurjchem-1701	261	30	110(100	110(100	NUM
eurjchem-1701	261	31	)	)	PUNCT
eurjchem-1701	261	32	,	,	PUNCT
eurjchem-1701	261	33	82(20	82(20	NUM
eurjchem-1701	261	34	)	)	PUNCT
eurjchem-1701	261	35	,	,	PUNCT
eurjchem-1701	261	36	57(25	57(25	PROPN
eurjchem-1701	261	37	)	)	PUNCT
eurjchem-1701	261	38	.	.	PUNCT
eurjchem-1701	262	1	anal	anal	PROPN
eurjchem-1701	262	2	.	.	PUNCT
eurjchem-1701	262	3	calcd	calcd	NOUN
eurjchem-1701	262	4	.	.	PUNCT
eurjchem-1701	263	1	for	for	ADP
eurjchem-1701	263	2	c14h12n4o2s3	c14h12n4o2s3	PROPN
eurjchem-1701	263	3	:	:	PUNCT
eurjchem-1701	263	4	c	c	X
eurjchem-1701	263	5	,	,	PUNCT
eurjchem-1701	263	6	46.14	46.14	NUM
eurjchem-1701	263	7	;	;	PUNCT
eurjchem-1701	263	8	h	h	NOUN
eurjchem-1701	263	9	,	,	PUNCT
eurjchem-1701	263	10	3.32	3.32	NUM
eurjchem-1701	263	11	;	;	PUNCT
eurjchem-1701	263	12	n	n	CCONJ
eurjchem-1701	263	13	,	,	PUNCT
eurjchem-1701	263	14	15.37	15.37	NUM
eurjchem-1701	263	15	.	.	PUNCT
eurjchem-1701	263	16	found	find	VERB
eurjchem-1701	263	17	:	:	PUNCT
eurjchem-1701	264	1	c	c	X
eurjchem-1701	264	2	,	,	PUNCT
eurjchem-1701	264	3	46.31	46.31	NUM
eurjchem-1701	264	4	;	;	PUNCT
eurjchem-1701	265	1	h	h	NOUN
eurjchem-1701	265	2	,	,	PUNCT
eurjchem-1701	265	3	3.20	3.20	NUM
eurjchem-1701	265	4	;	;	PUNCT
eurjchem-1701	265	5	n	n	CCONJ
eurjchem-1701	265	6	,	,	PUNCT
eurjchem-1701	265	7	15.26	15.26	NUM
eurjchem-1701	265	8	%	%	NOUN
eurjchem-1701	265	9	.	.	PUNCT
eurjchem-1701	266	1	2.4	2.4	NUM
eurjchem-1701	266	2	.	.	PUNCT
eurjchem-1701	267	1	antitumor	antitumor	NOUN
eurjchem-1701	267	2	activity	activity	NOUN
eurjchem-1701	267	3	test	test	NOUN
eurjchem-1701	267	4	tumor	tumor	NOUN
eurjchem-1701	267	5	cell	cell	NOUN
eurjchem-1701	267	6	growth	growth	NOUN
eurjchem-1701	267	7	assay	assay	VERB
eurjchem-1701	267	8	human	human	ADJ
eurjchem-1701	267	9	tumor	tumor	NOUN
eurjchem-1701	267	10	cell	cell	NOUN
eurjchem-1701	267	11	line	line	NOUN
eurjchem-1701	267	12	,	,	PUNCT
eurjchem-1701	267	13	mcf-7	mcf-7	PUNCT
eurjchem-1701	267	14	(	(	PUNCT
eurjchem-1701	267	15	breast	breast	NOUN
eurjchem-1701	267	16	adenocarcinoma	adenocarcinoma	NOUN
eurjchem-1701	267	17	)	)	PUNCT
eurjchem-1701	267	18	mcf-7	mcf-7	PUNCT
eurjchem-1701	267	19	was	be	AUX
eurjchem-1701	267	20	kindly	kindly	ADV
eurjchem-1701	267	21	provided	provide	VERB
eurjchem-1701	267	22	by	by	ADP
eurjchem-1701	267	23	the	the	DET
eurjchem-1701	267	24	national	national	PROPN
eurjchem-1701	267	25	cancer	cancer	PROPN
eurjchem-1701	267	26	institute	institute	PROPN
eurjchem-1701	267	27	(	(	PUNCT
eurjchem-1701	267	28	nci	nci	PROPN
eurjchem-1701	267	29	,	,	PUNCT
eurjchem-1701	267	30	cairo	cairo	PROPN
eurjchem-1701	267	31	,	,	PUNCT
eurjchem-1701	267	32	egypt	egypt	PROPN
eurjchem-1701	267	33	)	)	PUNCT
eurjchem-1701	267	34	.	.	PUNCT
eurjchem-1701	268	1	the	the	DET
eurjchem-1701	268	2	effects	effect	NOUN
eurjchem-1701	268	3	of	of	ADP
eurjchem-1701	268	4	compounds	compound	NOUN
eurjchem-1701	268	5	6	6	NUM
eurjchem-1701	268	6	,	,	PUNCT
eurjchem-1701	268	7	7	7	NUM
eurjchem-1701	268	8	,	,	PUNCT
eurjchem-1701	268	9	8	8	NUM
eurjchem-1701	268	10	,	,	PUNCT
eurjchem-1701	268	11	12	12	NUM
eurjchem-1701	268	12	,	,	PUNCT
eurjchem-1701	268	13	13	13	NUM
eurjchem-1701	268	14	,	,	PUNCT
eurjchem-1701	268	15	15	15	NUM
eurjchem-1701	268	16	,	,	PUNCT
eurjchem-1701	268	17	16	16	NUM
eurjchem-1701	268	18	and	and	CCONJ
eurjchem-1701	268	19	18	18	NUM
eurjchem-1701	268	20	on	on	ADP
eurjchem-1701	268	21	the	the	DET
eurjchem-1701	268	22	in	in	X
eurjchem-1701	268	23	vitro	vitro	X
eurjchem-1701	268	24	growth	growth	NOUN
eurjchem-1701	268	25	of	of	ADP
eurjchem-1701	268	26	human	human	ADJ
eurjchem-1701	268	27	tumor	tumor	NOUN
eurjchem-1701	268	28	cell	cell	NOUN
eurjchem-1701	268	29	line	line	NOUN
eurjchem-1701	268	30	were	be	AUX
eurjchem-1701	268	31	evaluated	evaluate	VERB
eurjchem-1701	268	32	according	accord	VERB
eurjchem-1701	268	33	to	to	ADP
eurjchem-1701	268	34	the	the	DET
eurjchem-1701	268	35	method	method	NOUN
eurjchem-1701	268	36	adopted	adopt	VERB
eurjchem-1701	268	37	by	by	ADP
eurjchem-1701	268	38	the	the	DET
eurjchem-1701	268	39	national	national	PROPN
eurjchem-1701	268	40	cancer	cancer	PROPN
eurjchem-1701	268	41	institute	institute	PROPN
eurjchem-1701	268	42	(	(	PUNCT
eurjchem-1701	268	43	nci	nci	PROPN
eurjchem-1701	268	44	,	,	PUNCT
eurjchem-1701	268	45	usa	usa	PROPN
eurjchem-1701	268	46	)	)	PUNCT
eurjchem-1701	269	1	[	[	X
eurjchem-1701	269	2	22	22	NUM
eurjchem-1701	269	3	-	-	SYM
eurjchem-1701	269	4	24	24	NUM
eurjchem-1701	269	5	]	]	PUNCT
eurjchem-1701	269	6	.	.	PUNCT
eurjchem-1701	270	1	2018	2018	NUM
eurjchem-1701	270	2	–	–	PUNCT
eurjchem-1701	270	3	european	european	ADJ
eurjchem-1701	270	4	journal	journal	NOUN
eurjchem-1701	270	5	of	of	ADP
eurjchem-1701	270	6	chemistry	chemistry	NOUN
eurjchem-1701	270	7	–	–	PUNCT
eurjchem-1701	270	8	cc	cc	NOUN
eurjchem-1701	270	9	by	by	ADP
eurjchem-1701	270	10	nc	nc	PROPN
eurjchem-1701	270	11	–	–	PUNCT
eurjchem-1701	270	12	doi	doi	NOUN
eurjchem-1701	270	13	:	:	PUNCT
eurjchem-1701	270	14	10.5155	10.5155	NUM
eurjchem-1701	270	15	/	/	SYM
eurjchem-1701	270	16	eurjchem.9.2.99	eurjchem.9.2.99	NUM
eurjchem-1701	270	17	-	-	PUNCT
eurjchem-1701	270	18	106.1701	106.1701	NUM
eurjchem-1701	270	19	haggam	haggam	NOUN
eurjchem-1701	270	20	et	et	PROPN
eurjchem-1701	270	21	al	al	PROPN
eurjchem-1701	270	22	.	.	PUNCT
eurjchem-1701	270	23	/	/	SYM
eurjchem-1701	270	24	european	european	PROPN
eurjchem-1701	270	25	journal	journal	PROPN
eurjchem-1701	270	26	of	of	ADP
eurjchem-1701	270	27	chemistry	chemistry	NOUN
eurjchem-1701	270	28	9	9	NUM
eurjchem-1701	270	29	(	(	PUNCT
eurjchem-1701	270	30	2	2	NUM
eurjchem-1701	270	31	)	)	PUNCT
eurjchem-1701	270	32	(	(	PUNCT
eurjchem-1701	270	33	2018	2018	NUM
eurjchem-1701	270	34	)	)	PUNCT
eurjchem-1701	270	35	99	99	NUM
eurjchem-1701	270	36	-	-	SYM
eurjchem-1701	270	37	106	106	NUM
eurjchem-1701	270	38	105	105	NUM
eurjchem-1701	270	39	table	table	NOUN
eurjchem-1701	270	40	1	1	NUM
eurjchem-1701	270	41	.	.	PUNCT
eurjchem-1701	271	1	the	the	DET
eurjchem-1701	271	2	inhibitory	inhibitory	ADJ
eurjchem-1701	271	3	activities	activity	NOUN
eurjchem-1701	271	4	of	of	ADP
eurjchem-1701	271	5	the	the	DET
eurjchem-1701	271	6	synthesized	synthesize	VERB
eurjchem-1701	271	7	compounds	compound	NOUN
eurjchem-1701	271	8	on	on	ADP
eurjchem-1701	271	9	the	the	DET
eurjchem-1701	271	10	growth	growth	NOUN
eurjchem-1701	271	11	of	of	ADP
eurjchem-1701	271	12	mcf-7	mcf-7	NOUN
eurjchem-1701	271	13	cell	cell	NOUN
eurjchem-1701	271	14	line	line	NOUN
eurjchem-1701	271	15	.	.	PUNCT
eurjchem-1701	272	1	compound	compound	PROPN
eurjchem-1701	272	2	gi50	gi50	PROPN
eurjchem-1701	272	3	(	(	PUNCT
eurjchem-1701	272	4	μg	μg	PROPN
eurjchem-1701	272	5	/	/	SYM
eurjchem-1701	272	6	l	l	NOUN
eurjchem-1701	272	7	)	)	PUNCT
eurjchem-1701	272	8	mcf-7	mcf-7	NUM
eurjchem-1701	272	9	8	8	NUM
eurjchem-1701	272	10	10.29±5.44	10.29±5.44	NUM
eurjchem-1701	272	11	12	12	NUM
eurjchem-1701	272	12	0.01±0.004	0.01±0.004	SYM
eurjchem-1701	272	13	13	13	NUM
eurjchem-1701	272	14	0.01±0.008	0.01±0.008	NOUN
eurjchem-1701	272	15	15	15	NUM
eurjchem-1701	272	16	0.01±0.001	0.01±0.001	NOUN
eurjchem-1701	272	17	16	16	NUM
eurjchem-1701	272	18	0.01±0.003	0.01±0.003	SYM
eurjchem-1701	272	19	18	18	NUM
eurjchem-1701	272	20	2.70±1.24	2.70±1.24	NUM
eurjchem-1701	272	21	doxorubicin	doxorubicin	NOUN
eurjchem-1701	272	22	0.04±0.008	0.04±0.008	PROPN
eurjchem-1701	272	23	table	table	NOUN
eurjchem-1701	272	24	2	2	NUM
eurjchem-1701	272	25	.	.	PUNCT
eurjchem-1701	272	26	evaluation	evaluation	NOUN
eurjchem-1701	272	27	of	of	ADP
eurjchem-1701	272	28	cytotoxicity	cytotoxicity	NOUN
eurjchem-1701	272	29	of	of	ADP
eurjchem-1701	272	30	the	the	DET
eurjchem-1701	272	31	obtained	obtain	VERB
eurjchem-1701	272	32	compounds	compound	NOUN
eurjchem-1701	272	33	against	against	ADP
eurjchem-1701	272	34	mcf-7	mcf-7	NOUN
eurjchem-1701	272	35	cell	cell	NOUN
eurjchem-1701	272	36	line	line	NOUN
eurjchem-1701	272	37	.	.	PUNCT
eurjchem-1701	273	1	compound	compound	NOUN
eurjchem-1701	273	2	viability	viability	NOUN
eurjchem-1701	273	3	rate	rate	NOUN
eurjchem-1701	273	4	(	(	PUNCT
eurjchem-1701	273	5	%	%	INTJ
eurjchem-1701	273	6	)	)	PUNCT
eurjchem-1701	273	7	ic50	ic50	PROPN
eurjchem-1701	273	8	(	(	PUNCT
eurjchem-1701	273	9	mg	mg	PROPN
eurjchem-1701	273	10	/	/	SYM
eurjchem-1701	273	11	ml	ml	NOUN
eurjchem-1701	273	12	)	)	PUNCT
eurjchem-1701	273	13	0.1	0.1	NUM
eurjchem-1701	273	14	μg	μg	PROPN
eurjchem-1701	273	15	/	/	SYM
eurjchem-1701	273	16	ml	ml	PROPN
eurjchem-1701	273	17	1	1	NUM
eurjchem-1701	273	18	μg	μg	NOUN
eurjchem-1701	273	19	/	/	SYM
eurjchem-1701	273	20	ml	ml	PROPN
eurjchem-1701	273	21	10	10	NUM
eurjchem-1701	273	22	μg	μg	NOUN
eurjchem-1701	273	23	/	/	SYM
eurjchem-1701	273	24	ml	ml	NOUN
eurjchem-1701	273	25	8	8	NUM
eurjchem-1701	273	26	87.26±6.29	87.26±6.29	NUM
eurjchem-1701	273	27	82.21±3.98	82.21±3.98	NUM
eurjchem-1701	273	28	80.23±5.56	80.23±5.56	NUM
eurjchem-1701	273	29	10.49±7.44	10.49±7.44	NUM
eurjchem-1701	273	30	12	12	NUM
eurjchem-1701	273	31	56.52±4.42	56.52±4.42	NUM
eurjchem-1701	273	32	50.89±5.50	50.89±5.50	PROPN
eurjchem-1701	273	33	55.23±3.90	55.23±3.90	NUM
eurjchem-1701	273	34	0.01±0.90	0.01±0.90	NOUN
eurjchem-1701	273	35	13	13	NUM
eurjchem-1701	273	36	54.62±4.53	54.62±4.53	PROPN
eurjchem-1701	273	37	58.09±6.50	58.09±6.50	NUM
eurjchem-1701	273	38	53.34±3.81	53.34±3.81	NUM
eurjchem-1701	273	39	0.01±0.50	0.01±0.50	NOUN
eurjchem-1701	273	40	15	15	NUM
eurjchem-1701	273	41	51.32±4.42	51.32±4.42	NUM
eurjchem-1701	273	42	55.89±5.50	55.89±5.50	NUM
eurjchem-1701	273	43	51.23±3.90	51.23±3.90	NUM
eurjchem-1701	273	44	0.01±0.008	0.01±0.008	PROPN
eurjchem-1701	273	45	16	16	NUM
eurjchem-1701	273	46	51.62±4.53	51.62±4.53	PROPN
eurjchem-1701	273	47	58.09±6.50	58.09±6.50	NUM
eurjchem-1701	273	48	51.34±3.81	51.34±3.81	NUM
eurjchem-1701	273	49	0.01±0.009	0.01±0.009	PROPN
eurjchem-1701	273	50	18	18	NUM
eurjchem-1701	273	51	93.26±4.19	93.26±4.19	NUM
eurjchem-1701	273	52	91.20±3.66	91.20±3.66	NUM
eurjchem-1701	273	53	82.09±5.71	82.09±5.71	NUM
eurjchem-1701	273	54	2.69±0.04	2.69±0.04	PROPN
eurjchem-1701	273	55	3	3	NUM
eurjchem-1701	273	56	.	.	PUNCT
eurjchem-1701	273	57	results	result	NOUN
eurjchem-1701	273	58	and	and	CCONJ
eurjchem-1701	273	59	discussion	discussion	NOUN
eurjchem-1701	273	60	3.1	3.1	NUM
eurjchem-1701	273	61	.	.	PUNCT
eurjchem-1701	274	1	chemistry	chemistry	NOUN
eurjchem-1701	274	2	this	this	DET
eurjchem-1701	274	3	research	research	NOUN
eurjchem-1701	274	4	aims	aim	VERB
eurjchem-1701	274	5	at	at	ADP
eurjchem-1701	274	6	presenting	present	VERB
eurjchem-1701	274	7	importance	importance	NOUN
eurjchem-1701	274	8	of	of	ADP
eurjchem-1701	274	9	isothiocyanates	isothiocyanate	NOUN
eurjchem-1701	274	10	as	as	ADP
eurjchem-1701	274	11	synthetic	synthetic	ADJ
eurjchem-1701	274	12	intermediate	intermediate	ADJ
eurjchem-1701	274	13	for	for	ADP
eurjchem-1701	274	14	building	build	VERB
eurjchem-1701	274	15	biologically	biologically	ADV
eurjchem-1701	274	16	active	active	ADJ
eurjchem-1701	274	17	heterocycles	heterocycle	NOUN
eurjchem-1701	274	18	[	[	X
eurjchem-1701	274	19	25,26	25,26	X
eurjchem-1701	274	20	]	]	X
eurjchem-1701	274	21	.	.	PUNCT
eurjchem-1701	275	1	to	to	PART
eurjchem-1701	275	2	begin	begin	VERB
eurjchem-1701	275	3	with	with	ADP
eurjchem-1701	275	4	addition	addition	NOUN
eurjchem-1701	275	5	of	of	ADP
eurjchem-1701	275	6	semicarbazide	semicarbazide	ADJ
eurjchem-1701	275	7	hydrochloride	hydrochloride	NOUN
eurjchem-1701	275	8	to	to	ADP
eurjchem-1701	275	9	thienoylisothiocyanate	thienoylisothiocyanate	NOUN
eurjchem-1701	275	10	(	(	PUNCT
eurjchem-1701	275	11	1	1	NUM
eurjchem-1701	275	12	)	)	PUNCT
eurjchem-1701	276	1	[	[	X
eurjchem-1701	276	2	27	27	NUM
eurjchem-1701	276	3	]	]	PUNCT
eurjchem-1701	276	4	in	in	ADP
eurjchem-1701	276	5	dioxane	dioxane	NOUN
eurjchem-1701	276	6	:	:	PUNCT
eurjchem-1701	276	7	water	water	NOUN
eurjchem-1701	276	8	(	(	PUNCT
eurjchem-1701	276	9	1:1	1:1	NUM
eurjchem-1701	276	10	,	,	PUNCT
eurjchem-1701	276	11	v	v	NOUN
eurjchem-1701	276	12	:	:	SYM
eurjchem-1701	276	13	v	v	NOUN
eurjchem-1701	276	14	)	)	PUNCT
eurjchem-1701	276	15	(	(	PUNCT
eurjchem-1701	276	16	50	50	NUM
eurjchem-1701	276	17	ml	ml	NOUN
eurjchem-1701	276	18	)	)	PUNCT
eurjchem-1701	276	19	with	with	ADP
eurjchem-1701	276	20	stirring	stir	VERB
eurjchem-1701	276	21	at	at	ADP
eurjchem-1701	276	22	room	room	NOUN
eurjchem-1701	276	23	temperature	temperature	NOUN
eurjchem-1701	276	24	for	for	ADP
eurjchem-1701	276	25	1	1	NUM
eurjchem-1701	276	26	h	h	NOUN
eurjchem-1701	276	27	afforded	afford	VERB
eurjchem-1701	276	28	thiosemicarbazide	thiosemicarbazide	ADJ
eurjchem-1701	276	29	derivative	derivative	ADJ
eurjchem-1701	276	30	2	2	NUM
eurjchem-1701	276	31	as	as	ADP
eurjchem-1701	276	32	a	a	DET
eurjchem-1701	276	33	result	result	NOUN
eurjchem-1701	276	34	of	of	ADP
eurjchem-1701	276	35	nucleophilic	nucleophilic	ADJ
eurjchem-1701	276	36	addition	addition	NOUN
eurjchem-1701	276	37	to	to	ADP
eurjchem-1701	276	38	the	the	DET
eurjchem-1701	276	39	electrophilic	electrophilic	ADJ
eurjchem-1701	276	40	carbon	carbon	NOUN
eurjchem-1701	276	41	of	of	ADP
eurjchem-1701	276	42	the	the	DET
eurjchem-1701	276	43	isothiocyanate	isothiocyanate	ADJ
eurjchem-1701	276	44	group	group	NOUN
eurjchem-1701	276	45	.	.	PUNCT
eurjchem-1701	277	1	an	an	DET
eurjchem-1701	277	2	intramolecular	intramolecular	ADJ
eurjchem-1701	277	3	basic	basic	ADJ
eurjchem-1701	277	4	cyclization	cyclization	NOUN
eurjchem-1701	277	5	of	of	ADP
eurjchem-1701	277	6	thiophene	thiophene	NOUN
eurjchem-1701	277	7	derivative	derivative	ADJ
eurjchem-1701	277	8	2	2	NUM
eurjchem-1701	277	9	in	in	ADP
eurjchem-1701	277	10	sodium	sodium	NOUN
eurjchem-1701	277	11	ethoxide	ethoxide	NOUN
eurjchem-1701	277	12	resulted	result	VERB
eurjchem-1701	277	13	in	in	ADP
eurjchem-1701	277	14	oxadiazine	oxadiazine	NOUN
eurjchem-1701	277	15	nuclus	nuclus	ADJ
eurjchem-1701	277	16	3	3	NUM
eurjchem-1701	277	17	in	in	ADP
eurjchem-1701	277	18	89	89	NUM
eurjchem-1701	277	19	%	%	NOUN
eurjchem-1701	277	20	yield	yield	NOUN
eurjchem-1701	277	21	(	(	PUNCT
eurjchem-1701	277	22	scheme	scheme	NOUN
eurjchem-1701	277	23	1	1	NUM
eurjchem-1701	277	24	)	)	PUNCT
eurjchem-1701	277	25	.	.	PUNCT
eurjchem-1701	278	1	moreover	moreover	ADV
eurjchem-1701	278	2	,	,	PUNCT
eurjchem-1701	278	3	addition	addition	NOUN
eurjchem-1701	278	4	of	of	ADP
eurjchem-1701	278	5	phenylhydrazine	phenylhydrazine	NOUN
eurjchem-1701	278	6	to	to	ADP
eurjchem-1701	278	7	the	the	DET
eurjchem-1701	278	8	heteroallene	heteroallene	NOUN
eurjchem-1701	278	9	1	1	NUM
eurjchem-1701	278	10	led	lead	VERB
eurjchem-1701	278	11	to	to	ADP
eurjchem-1701	278	12	formation	formation	NOUN
eurjchem-1701	278	13	of	of	ADP
eurjchem-1701	278	14	the	the	DET
eurjchem-1701	278	15	expected	expect	VERB
eurjchem-1701	278	16	triazole	triazole	NOUN
eurjchem-1701	278	17	4	4	NUM
eurjchem-1701	278	18	in	in	ADP
eurjchem-1701	278	19	63	63	NUM
eurjchem-1701	278	20	%	%	NOUN
eurjchem-1701	278	21	yield	yield	NOUN
eurjchem-1701	278	22	after	after	ADP
eurjchem-1701	278	23	loss	loss	NOUN
eurjchem-1701	278	24	of	of	ADP
eurjchem-1701	278	25	h2o	h2o	PROPN
eurjchem-1701	278	26	molecule	molecule	NOUN
eurjchem-1701	278	27	(	(	PUNCT
eurjchem-1701	278	28	scheme	scheme	NOUN
eurjchem-1701	278	29	1	1	NUM
eurjchem-1701	278	30	)	)	PUNCT
eurjchem-1701	278	31	.	.	PUNCT
eurjchem-1701	279	1	the	the	DET
eurjchem-1701	279	2	new	new	ADJ
eurjchem-1701	279	3	structures	structure	NOUN
eurjchem-1701	279	4	of	of	ADP
eurjchem-1701	279	5	the	the	DET
eurjchem-1701	279	6	prepared	prepare	VERB
eurjchem-1701	279	7	compounds	compound	NOUN
eurjchem-1701	279	8	were	be	AUX
eurjchem-1701	279	9	elucidated	elucidate	VERB
eurjchem-1701	279	10	on	on	ADP
eurjchem-1701	279	11	the	the	DET
eurjchem-1701	279	12	bases	basis	NOUN
eurjchem-1701	279	13	of	of	ADP
eurjchem-1701	279	14	their	their	PRON
eurjchem-1701	279	15	spectroscopic	spectroscopic	ADJ
eurjchem-1701	279	16	data	datum	NOUN
eurjchem-1701	279	17	.	.	PUNCT
eurjchem-1701	280	1	as	as	ADP
eurjchem-1701	280	2	an	an	DET
eurjchem-1701	280	3	example	example	NOUN
eurjchem-1701	280	4	,	,	PUNCT
eurjchem-1701	280	5	the	the	DET
eurjchem-1701	280	6	ir	ir	PROPN
eurjchem-1701	280	7	spectrum	spectrum	NOUN
eurjchem-1701	280	8	of	of	ADP
eurjchem-1701	280	9	oxadiazine	oxadiazine	NOUN
eurjchem-1701	280	10	derivative	derivative	ADJ
eurjchem-1701	280	11	3	3	NUM
eurjchem-1701	280	12	exhibited	exhibit	VERB
eurjchem-1701	280	13	characteristic	characteristic	ADJ
eurjchem-1701	280	14	absorption	absorption	NOUN
eurjchem-1701	280	15	bands	band	NOUN
eurjchem-1701	280	16	at	at	ADP
eurjchem-1701	280	17	3411	3411	NUM
eurjchem-1701	280	18	,	,	PUNCT
eurjchem-1701	280	19	3325	3325	NUM
eurjchem-1701	280	20	,	,	PUNCT
eurjchem-1701	280	21	1599	1599	NUM
eurjchem-1701	280	22	and	and	CCONJ
eurjchem-1701	280	23	1235	1235	NUM
eurjchem-1701	280	24	cm-1	cm-1	X
eurjchem-1701	280	25	for	for	ADP
eurjchem-1701	280	26	nh	nh	PROPN
eurjchem-1701	280	27	,	,	PUNCT
eurjchem-1701	280	28	nh2	nh2	PROPN
eurjchem-1701	280	29	,	,	PUNCT
eurjchem-1701	280	30	c	c	NOUN
eurjchem-1701	280	31	=	=	SYM
eurjchem-1701	280	32	n	n	NOUN
eurjchem-1701	280	33	and	and	CCONJ
eurjchem-1701	280	34	c	c	NOUN
eurjchem-1701	280	35	=	=	SYM
eurjchem-1701	280	36	s	s	NOUN
eurjchem-1701	280	37	,	,	PUNCT
eurjchem-1701	280	38	respectively	respectively	ADV
eurjchem-1701	280	39	.	.	PUNCT
eurjchem-1701	281	1	in	in	ADP
eurjchem-1701	281	2	addition	addition	NOUN
eurjchem-1701	281	3	to	to	ADP
eurjchem-1701	281	4	,	,	PUNCT
eurjchem-1701	281	5	absence	absence	NOUN
eurjchem-1701	281	6	of	of	ADP
eurjchem-1701	281	7	carbonyl	carbonyl	NOUN
eurjchem-1701	281	8	stretching	stretching	NOUN
eurjchem-1701	281	9	peak	peak	NOUN
eurjchem-1701	281	10	is	be	AUX
eurjchem-1701	281	11	observed	observe	VERB
eurjchem-1701	281	12	.	.	PUNCT
eurjchem-1701	282	1	the	the	DET
eurjchem-1701	282	2	1h	1h	NUM
eurjchem-1701	282	3	nmr	nmr	NOUN
eurjchem-1701	282	4	of	of	ADP
eurjchem-1701	282	5	compound	compound	NOUN
eurjchem-1701	282	6	3	3	NUM
eurjchem-1701	282	7	showed	show	VERB
eurjchem-1701	282	8	two	two	NUM
eurjchem-1701	282	9	singlets	singlet	NOUN
eurjchem-1701	282	10	with	with	ADP
eurjchem-1701	282	11	different	different	ADJ
eurjchem-1701	282	12	integration	integration	NOUN
eurjchem-1701	282	13	at	at	ADP
eurjchem-1701	282	14	δ	δ	PROPN
eurjchem-1701	282	15	13.91	13.91	NUM
eurjchem-1701	282	16	and	and	CCONJ
eurjchem-1701	282	17	13.61	13.61	NUM
eurjchem-1701	282	18	ppm	ppm	NOUN
eurjchem-1701	282	19	for	for	ADP
eurjchem-1701	282	20	nh	nh	PROPN
eurjchem-1701	282	21	and	and	CCONJ
eurjchem-1701	282	22	nh2	nh2	PROPN
eurjchem-1701	282	23	protons	proton	NOUN
eurjchem-1701	282	24	,	,	PUNCT
eurjchem-1701	282	25	respecttively	respecttively	ADV
eurjchem-1701	282	26	.	.	PUNCT
eurjchem-1701	283	1	there	there	PRON
eurjchem-1701	283	2	is	be	VERB
eurjchem-1701	283	3	a	a	DET
eurjchem-1701	283	4	multiplet	multiplet	NOUN
eurjchem-1701	283	5	in	in	ADP
eurjchem-1701	283	6	between	between	ADP
eurjchem-1701	283	7	δ	δ	PROPN
eurjchem-1701	283	8	7.75	7.75	NUM
eurjchem-1701	283	9	-	-	SYM
eurjchem-1701	283	10	7.19	7.19	NUM
eurjchem-1701	283	11	ppm	ppm	NOUN
eurjchem-1701	283	12	for	for	ADP
eurjchem-1701	283	13	three	three	NUM
eurjchem-1701	283	14	protons	proton	NOUN
eurjchem-1701	283	15	of	of	ADP
eurjchem-1701	283	16	the	the	DET
eurjchem-1701	283	17	thiophene	thiophene	NOUN
eurjchem-1701	283	18	ring	ring	NOUN
eurjchem-1701	283	19	.	.	PUNCT
eurjchem-1701	284	1	disappearance	disappearance	VERB
eurjchem-1701	284	2	the	the	DET
eurjchem-1701	284	3	two	two	NUM
eurjchem-1701	284	4	peaks	peak	NOUN
eurjchem-1701	284	5	at	at	ADP
eurjchem-1701	284	6	δ	δ	PROPN
eurjchem-1701	284	7	13.91	13.91	NUM
eurjchem-1701	284	8	and	and	CCONJ
eurjchem-1701	284	9	13.61	13.61	NUM
eurjchem-1701	284	10	ppm	ppm	NOUN
eurjchem-1701	284	11	in	in	ADP
eurjchem-1701	284	12	d2o	d2o	NOUN
eurjchem-1701	284	13	spectrum	spectrum	NOUN
eurjchem-1701	284	14	of	of	ADP
eurjchem-1701	284	15	compound	compound	NOUN
eurjchem-1701	284	16	3	3	NUM
eurjchem-1701	284	17	emphasized	emphasize	VERB
eurjchem-1701	284	18	that	that	SCONJ
eurjchem-1701	284	19	the	the	DET
eurjchem-1701	284	20	nh	nh	PROPN
eurjchem-1701	284	21	and	and	CCONJ
eurjchem-1701	284	22	nh2	nh2	PROPN
eurjchem-1701	284	23	protons	proton	NOUN
eurjchem-1701	284	24	were	be	AUX
eurjchem-1701	284	25	exchangeable	exchangeable	ADJ
eurjchem-1701	284	26	with	with	ADP
eurjchem-1701	284	27	d2o	d2o	PROPN
eurjchem-1701	284	28	and	and	CCONJ
eurjchem-1701	284	29	this	this	PRON
eurjchem-1701	284	30	is	be	AUX
eurjchem-1701	284	31	proof	proof	NOUN
eurjchem-1701	284	32	for	for	ADP
eurjchem-1701	284	33	the	the	DET
eurjchem-1701	284	34	correct	correct	ADJ
eurjchem-1701	284	35	suggested	suggest	VERB
eurjchem-1701	284	36	structure	structure	NOUN
eurjchem-1701	284	37	.	.	PUNCT
eurjchem-1701	285	1	also	also	ADV
eurjchem-1701	285	2	,	,	PUNCT
eurjchem-1701	285	3	the	the	DET
eurjchem-1701	285	4	mass	mass	ADJ
eurjchem-1701	285	5	spectrometry	spectrometry	NOUN
eurjchem-1701	285	6	of	of	ADP
eurjchem-1701	285	7	compound	compound	NOUN
eurjchem-1701	285	8	3	3	NUM
eurjchem-1701	285	9	is	be	AUX
eurjchem-1701	285	10	in	in	ADP
eurjchem-1701	285	11	agreement	agreement	NOUN
eurjchem-1701	285	12	with	with	ADP
eurjchem-1701	285	13	its	its	PRON
eurjchem-1701	285	14	structure	structure	NOUN
eurjchem-1701	285	15	as	as	ADV
eurjchem-1701	285	16	well	well	ADV
eurjchem-1701	285	17	as	as	ADP
eurjchem-1701	285	18	its	its	PRON
eurjchem-1701	285	19	molecular	molecular	ADJ
eurjchem-1701	285	20	weight	weight	NOUN
eurjchem-1701	285	21	.	.	PUNCT
eurjchem-1701	286	1	the	the	DET
eurjchem-1701	286	2	1h	1h	NUM
eurjchem-1701	286	3	nmr	nmr	NOUN
eurjchem-1701	286	4	spectrum	spectrum	NOUN
eurjchem-1701	286	5	of	of	ADP
eurjchem-1701	286	6	compound	compound	NOUN
eurjchem-1701	286	7	4	4	NUM
eurjchem-1701	286	8	revealed	reveal	VERB
eurjchem-1701	286	9	a	a	DET
eurjchem-1701	286	10	sharp	sharp	ADJ
eurjchem-1701	286	11	singlet	singlet	NOUN
eurjchem-1701	286	12	at	at	ADP
eurjchem-1701	286	13	δ	δ	PROPN
eurjchem-1701	286	14	10.37	10.37	NUM
eurjchem-1701	286	15	ppm	ppm	NOUN
eurjchem-1701	286	16	for	for	ADP
eurjchem-1701	286	17	nh	nh	PROPN
eurjchem-1701	286	18	proton	proton	NOUN
eurjchem-1701	286	19	which	which	PRON
eurjchem-1701	286	20	was	be	AUX
eurjchem-1701	286	21	d2o	d2o	NOUN
eurjchem-1701	286	22	exchangeable	exchangeable	ADJ
eurjchem-1701	286	23	.	.	PUNCT
eurjchem-1701	287	1	addition	addition	NOUN
eurjchem-1701	287	2	of	of	ADP
eurjchem-1701	287	3	phenylhydrazine	phenylhydrazine	ADJ
eurjchem-1701	287	4	hydrochloride	hydrochloride	NOUN
eurjchem-1701	287	5	to	to	ADP
eurjchem-1701	287	6	thiophene2	thiophene2	NOUN
eurjchem-1701	287	7	-	-	PUNCT
eurjchem-1701	287	8	carbonyl	carbonyl	NOUN
eurjchem-1701	287	9	isothiocyanate	isothiocyanate	NOUN
eurjchem-1701	287	10	(	(	PUNCT
eurjchem-1701	287	11	1	1	NUM
eurjchem-1701	287	12	)	)	PUNCT
eurjchem-1701	287	13	in	in	ADP
eurjchem-1701	287	14	dioxane	dioxane	NOUN
eurjchem-1701	287	15	:	:	PUNCT
eurjchem-1701	287	16	water	water	NOUN
eurjchem-1701	287	17	(	(	PUNCT
eurjchem-1701	287	18	1:1	1:1	NUM
eurjchem-1701	287	19	,	,	PUNCT
eurjchem-1701	287	20	v	v	NOUN
eurjchem-1701	287	21	:	:	SYM
eurjchem-1701	287	22	v	v	NOUN
eurjchem-1701	287	23	)	)	PUNCT
eurjchem-1701	287	24	produced	produce	VERB
eurjchem-1701	287	25	thiosemicarbazide	thiosemicarbazide	ADV
eurjchem-1701	287	26	5	5	NUM
eurjchem-1701	288	1	[	[	SYM
eurjchem-1701	288	2	23	23	NUM
eurjchem-1701	288	3	-	-	SYM
eurjchem-1701	288	4	25	25	NUM
eurjchem-1701	288	5	]	]	PUNCT
eurjchem-1701	288	6	.	.	PUNCT
eurjchem-1701	289	1	the	the	DET
eurjchem-1701	289	2	synthesis	synthesis	NOUN
eurjchem-1701	289	3	of	of	ADP
eurjchem-1701	289	4	thiadiazine	thiadiazine	NOUN
eurjchem-1701	289	5	derivative	derivative	ADJ
eurjchem-1701	289	6	6	6	NUM
eurjchem-1701	289	7	in	in	ADP
eurjchem-1701	289	8	61	61	NUM
eurjchem-1701	289	9	%	%	NOUN
eurjchem-1701	289	10	yield	yield	NOUN
eurjchem-1701	289	11	was	be	AUX
eurjchem-1701	289	12	achieved	achieve	VERB
eurjchem-1701	289	13	via	via	ADP
eurjchem-1701	289	14	one	one	NUM
eurjchem-1701	289	15	pot	pot	NOUN
eurjchem-1701	289	16	three	three	NUM
eurjchem-1701	289	17	component	component	NOUN
eurjchem-1701	289	18	reaction	reaction	NOUN
eurjchem-1701	289	19	of	of	ADP
eurjchem-1701	289	20	compound	compound	NOUN
eurjchem-1701	289	21	5	5	NUM
eurjchem-1701	289	22	,	,	PUNCT
eurjchem-1701	289	23	maleic	maleic	ADJ
eurjchem-1701	289	24	anhydride	anhydride	NOUN
eurjchem-1701	289	25	and	and	CCONJ
eurjchem-1701	289	26	triethyl	triethyl	NOUN
eurjchem-1701	289	27	amine	amine	PROPN
eurjchem-1701	289	28	in	in	ADP
eurjchem-1701	289	29	dmf	dmf	PROPN
eurjchem-1701	289	30	(	(	PUNCT
eurjchem-1701	289	31	scheme	scheme	NOUN
eurjchem-1701	289	32	2	2	NUM
eurjchem-1701	289	33	)	)	PUNCT
eurjchem-1701	289	34	.	.	PUNCT
eurjchem-1701	290	1	a	a	DET
eurjchem-1701	290	2	mixture	mixture	NOUN
eurjchem-1701	290	3	of	of	ADP
eurjchem-1701	290	4	ethyl	ethyl	PROPN
eurjchem-1701	290	5	chloroacetate	chloroacetate	NOUN
eurjchem-1701	290	6	and	and	CCONJ
eurjchem-1701	290	7	thiophene-2	thiophene-2	NUM
eurjchem-1701	290	8	-	-	PUNCT
eurjchem-1701	290	9	carboxamide	carboxamide	NOUN
eurjchem-1701	290	10	hydrochloride	hydrochloride	NOUN
eurjchem-1701	290	11	5	5	NUM
eurjchem-1701	290	12	was	be	AUX
eurjchem-1701	290	13	heated	heat	VERB
eurjchem-1701	290	14	for	for	SCONJ
eurjchem-1701	290	15	6	6	NUM
eurjchem-1701	290	16	h	h	NOUN
eurjchem-1701	290	17	to	to	PART
eurjchem-1701	290	18	yield	yield	VERB
eurjchem-1701	290	19	thiadiazine	thiadiazine	NOUN
eurjchem-1701	290	20	7	7	NUM
eurjchem-1701	290	21	in	in	ADP
eurjchem-1701	290	22	79	79	NUM
eurjchem-1701	290	23	%	%	NOUN
eurjchem-1701	290	24	yield	yield	NOUN
eurjchem-1701	290	25	.	.	PUNCT
eurjchem-1701	291	1	upon	upon	SCONJ
eurjchem-1701	291	2	heating	heat	VERB
eurjchem-1701	291	3	5	5	NUM
eurjchem-1701	291	4	with	with	ADP
eurjchem-1701	291	5	sodium	sodium	NOUN
eurjchem-1701	291	6	ethoxide	ethoxide	NOUN
eurjchem-1701	291	7	for	for	ADP
eurjchem-1701	291	8	2	2	NUM
eurjchem-1701	291	9	h	h	NOUN
eurjchem-1701	291	10	,	,	PUNCT
eurjchem-1701	291	11	the	the	DET
eurjchem-1701	291	12	triazole	triazole	NOUN
eurjchem-1701	291	13	8	8	NUM
eurjchem-1701	291	14	was	be	AUX
eurjchem-1701	291	15	obtained	obtain	VERB
eurjchem-1701	291	16	in	in	ADP
eurjchem-1701	291	17	95	95	NUM
eurjchem-1701	291	18	%	%	NOUN
eurjchem-1701	291	19	yield	yield	NOUN
eurjchem-1701	291	20	as	as	ADP
eurjchem-1701	291	21	in	in	ADP
eurjchem-1701	291	22	scheme	scheme	NOUN
eurjchem-1701	291	23	2	2	NUM
eurjchem-1701	291	24	.	.	PUNCT
eurjchem-1701	292	1	the	the	DET
eurjchem-1701	292	2	ir	ir	PROPN
eurjchem-1701	292	3	spectrum	spectrum	NOUN
eurjchem-1701	292	4	of	of	ADP
eurjchem-1701	292	5	compound	compound	NOUN
eurjchem-1701	292	6	8	8	NUM
eurjchem-1701	292	7	showed	show	VERB
eurjchem-1701	292	8	strong	strong	ADJ
eurjchem-1701	292	9	bands	band	NOUN
eurjchem-1701	292	10	at	at	ADP
eurjchem-1701	292	11	3424	3424	NUM
eurjchem-1701	292	12	,	,	PUNCT
eurjchem-1701	292	13	1597	1597	NUM
eurjchem-1701	292	14	and	and	CCONJ
eurjchem-1701	292	15	1252	1252	NUM
eurjchem-1701	292	16	cm-1	cm-1	X
eurjchem-1701	292	17	for	for	ADP
eurjchem-1701	292	18	nh	nh	PROPN
eurjchem-1701	292	19	,	,	PUNCT
eurjchem-1701	292	20	c	c	PROPN
eurjchem-1701	292	21	=	=	NOUN
eurjchem-1701	292	22	n	n	NOUN
eurjchem-1701	292	23	and	and	CCONJ
eurjchem-1701	292	24	c	c	NOUN
eurjchem-1701	292	25	=	=	SYM
eurjchem-1701	292	26	s	s	NOUN
eurjchem-1701	292	27	,	,	PUNCT
eurjchem-1701	292	28	respectively	respectively	ADV
eurjchem-1701	292	29	.	.	PUNCT
eurjchem-1701	293	1	the	the	DET
eurjchem-1701	293	2	1h	1h	NUM
eurjchem-1701	293	3	nmr	nmr	NOUN
eurjchem-1701	293	4	spectrum	spectrum	NOUN
eurjchem-1701	293	5	of	of	ADP
eurjchem-1701	293	6	triazole	triazole	NOUN
eurjchem-1701	293	7	8	8	NUM
eurjchem-1701	293	8	displayed	display	VERB
eurjchem-1701	293	9	a	a	DET
eurjchem-1701	293	10	singlet	singlet	NOUN
eurjchem-1701	293	11	at	at	ADP
eurjchem-1701	293	12	δ	δ	PROPN
eurjchem-1701	293	13	14.41	14.41	NUM
eurjchem-1701	293	14	ppm	ppm	NOUN
eurjchem-1701	293	15	for	for	ADP
eurjchem-1701	293	16	nh	nh	PROPN
eurjchem-1701	293	17	proton	proton	NOUN
eurjchem-1701	293	18	which	which	PRON
eurjchem-1701	293	19	was	be	AUX
eurjchem-1701	293	20	exchangeable	exchangeable	ADJ
eurjchem-1701	293	21	with	with	ADP
eurjchem-1701	293	22	d2o	d2o	NOUN
eurjchem-1701	293	23	as	as	ADV
eurjchem-1701	293	24	well	well	ADV
eurjchem-1701	293	25	.	.	PUNCT
eurjchem-1701	294	1	a	a	DET
eurjchem-1701	294	2	multiplet	multiplet	NOUN
eurjchem-1701	294	3	peak	peak	NOUN
eurjchem-1701	294	4	is	be	AUX
eurjchem-1701	294	5	at	at	ADP
eurjchem-1701	294	6	δ	δ	PROPN
eurjchem-1701	294	7	8.06	8.06	NUM
eurjchem-1701	294	8	-	-	SYM
eurjchem-1701	294	9	7.18	7.18	NUM
eurjchem-1701	294	10	ppm	ppm	NOUN
eurjchem-1701	294	11	for	for	ADP
eurjchem-1701	294	12	aromatic	aromatic	ADJ
eurjchem-1701	294	13	protons	proton	NOUN
eurjchem-1701	294	14	.	.	PUNCT
eurjchem-1701	295	1	the	the	DET
eurjchem-1701	295	2	mass	mass	ADJ
eurjchem-1701	295	3	spectrometry	spectrometry	NOUN
eurjchem-1701	295	4	of	of	ADP
eurjchem-1701	295	5	compound	compound	NOUN
eurjchem-1701	295	6	8	8	NUM
eurjchem-1701	295	7	is	be	AUX
eurjchem-1701	295	8	in	in	ADP
eurjchem-1701	295	9	agreement	agreement	NOUN
eurjchem-1701	295	10	with	with	ADP
eurjchem-1701	295	11	its	its	PRON
eurjchem-1701	295	12	suggested	suggest	VERB
eurjchem-1701	295	13	structure	structure	NOUN
eurjchem-1701	295	14	.	.	PUNCT
eurjchem-1701	296	1	the	the	DET
eurjchem-1701	296	2	suggested	suggest	VERB
eurjchem-1701	296	3	mechanism	mechanism	NOUN
eurjchem-1701	296	4	for	for	ADP
eurjchem-1701	296	5	establishment	establishment	NOUN
eurjchem-1701	296	6	of	of	ADP
eurjchem-1701	296	7	thienoylthiadiazine	thienoylthiadiazine	NOUN
eurjchem-1701	296	8	6	6	NUM
eurjchem-1701	296	9	showed	show	VERB
eurjchem-1701	296	10	that	that	SCONJ
eurjchem-1701	296	11	formation	formation	NOUN
eurjchem-1701	296	12	of	of	ADP
eurjchem-1701	296	13	acyclic	acyclic	ADJ
eurjchem-1701	296	14	thienoylimine	thienoylimine	NOUN
eurjchem-1701	296	15	intermediate	intermediate	ADJ
eurjchem-1701	296	16	9	9	NUM
eurjchem-1701	296	17	.	.	PUNCT
eurjchem-1701	296	18	subsequently	subsequently	ADV
eurjchem-1701	296	19	,	,	PUNCT
eurjchem-1701	296	20	the	the	DET
eurjchem-1701	296	21	intermediate	intermediate	ADJ
eurjchem-1701	296	22	9	9	NUM
eurjchem-1701	296	23	underwent	undergo	VERB
eurjchem-1701	296	24	an	an	DET
eurjchem-1701	296	25	intramolecular	intramolecular	ADJ
eurjchem-1701	296	26	nucleophilic	nucleophilic	ADJ
eurjchem-1701	296	27	cyclization	cyclization	NOUN
eurjchem-1701	296	28	to	to	PART
eurjchem-1701	296	29	form	form	VERB
eurjchem-1701	296	30	thiadiazine	thiadiazine	VERB
eurjchem-1701	296	31	derivative	derivative	ADJ
eurjchem-1701	296	32	10	10	NUM
eurjchem-1701	296	33	that	that	PRON
eurjchem-1701	296	34	was	be	AUX
eurjchem-1701	296	35	dehydrated	dehydrate	VERB
eurjchem-1701	296	36	giving	give	VERB
eurjchem-1701	296	37	thienoylthiadiazine	thienoylthiadiazine	NOUN
eurjchem-1701	296	38	structure	structure	NOUN
eurjchem-1701	296	39	6	6	NUM
eurjchem-1701	296	40	(	(	PUNCT
eurjchem-1701	296	41	scheme	scheme	NOUN
eurjchem-1701	296	42	3	3	NUM
eurjchem-1701	296	43	)	)	PUNCT
eurjchem-1701	296	44	.	.	PUNCT
eurjchem-1701	297	1	thiosemicarbazide	thiosemicarbazide	VERB
eurjchem-1701	297	2	derivative	derivative	ADJ
eurjchem-1701	297	3	11	11	NUM
eurjchem-1701	297	4	was	be	AUX
eurjchem-1701	297	5	synthesized	synthesize	VERB
eurjchem-1701	297	6	by	by	ADP
eurjchem-1701	297	7	the	the	DET
eurjchem-1701	297	8	addition	addition	NOUN
eurjchem-1701	297	9	of	of	ADP
eurjchem-1701	297	10	nicotinic	nicotinic	ADJ
eurjchem-1701	297	11	hydrazide	hydrazide	NOUN
eurjchem-1701	297	12	to	to	ADP
eurjchem-1701	297	13	thiophene-2	thiophene-2	NUM
eurjchem-1701	297	14	-	-	PUNCT
eurjchem-1701	297	15	carbonyl	carbonyl	NOUN
eurjchem-1701	297	16	isothiocyanate	isothiocyanate	NOUN
eurjchem-1701	297	17	(	(	PUNCT
eurjchem-1701	297	18	1	1	NUM
eurjchem-1701	297	19	)	)	PUNCT
eurjchem-1701	297	20	in	in	ADP
eurjchem-1701	297	21	dioxane	dioxane	NOUN
eurjchem-1701	297	22	as	as	SCONJ
eurjchem-1701	297	23	outlined	outline	VERB
eurjchem-1701	297	24	in	in	ADP
eurjchem-1701	297	25	(	(	PUNCT
eurjchem-1701	297	26	scheme	scheme	NOUN
eurjchem-1701	297	27	4	4	NUM
eurjchem-1701	297	28	)	)	PUNCT
eurjchem-1701	298	1	[	[	X
eurjchem-1701	298	2	23	23	NUM
eurjchem-1701	298	3	-	-	SYM
eurjchem-1701	298	4	25	25	NUM
eurjchem-1701	298	5	]	]	PUNCT
eurjchem-1701	298	6	.	.	PUNCT
eurjchem-1701	299	1	depending	depend	VERB
eurjchem-1701	299	2	on	on	ADP
eurjchem-1701	299	3	reaction	reaction	NOUN
eurjchem-1701	299	4	condition	condition	NOUN
eurjchem-1701	299	5	compound	compound	NOUN
eurjchem-1701	299	6	11	11	NUM
eurjchem-1701	299	7	underwent	undergo	VERB
eurjchem-1701	299	8	several	several	ADJ
eurjchem-1701	299	9	kinds	kind	NOUN
eurjchem-1701	299	10	of	of	ADP
eurjchem-1701	299	11	heterocyclizations	heterocyclization	NOUN
eurjchem-1701	299	12	.	.	PUNCT
eurjchem-1701	300	1	so	so	ADV
eurjchem-1701	300	2	,	,	PUNCT
eurjchem-1701	300	3	acid	acid	NOUN
eurjchem-1701	300	4	mediated	mediate	VERB
eurjchem-1701	300	5	cyclization	cyclization	NOUN
eurjchem-1701	300	6	of	of	ADP
eurjchem-1701	300	7	compound	compound	NOUN
eurjchem-1701	300	8	11	11	NUM
eurjchem-1701	300	9	resulted	result	VERB
eurjchem-1701	300	10	in	in	ADP
eurjchem-1701	300	11	thiadiazole	thiadiazole	NOUN
eurjchem-1701	300	12	ring	ring	NOUN
eurjchem-1701	300	13	12	12	NUM
eurjchem-1701	300	14	in	in	ADP
eurjchem-1701	300	15	95	95	NUM
eurjchem-1701	300	16	%	%	NOUN
eurjchem-1701	300	17	yield	yield	NOUN
eurjchem-1701	300	18	.	.	PUNCT
eurjchem-1701	301	1	heating	heating	NOUN
eurjchem-1701	301	2	of	of	ADP
eurjchem-1701	301	3	compound	compound	NOUN
eurjchem-1701	301	4	11	11	NUM
eurjchem-1701	301	5	with	with	ADP
eurjchem-1701	301	6	lead	lead	ADJ
eurjchem-1701	301	7	acetate	acetate	NOUN
eurjchem-1701	301	8	in	in	ADP
eurjchem-1701	301	9	acetic	acetic	ADJ
eurjchem-1701	301	10	acid	acid	NOUN
eurjchem-1701	301	11	produced	produce	VERB
eurjchem-1701	301	12	triazole	triazole	ADJ
eurjchem-1701	301	13	derivative	derivative	ADJ
eurjchem-1701	301	14	cyclization	cyclization	NOUN
eurjchem-1701	301	15	13	13	NUM
eurjchem-1701	301	16	in	in	ADP
eurjchem-1701	301	17	83	83	NUM
eurjchem-1701	301	18	%	%	NOUN
eurjchem-1701	301	19	yield	yield	NOUN
eurjchem-1701	301	20	.	.	PUNCT
eurjchem-1701	302	1	on	on	ADP
eurjchem-1701	302	2	the	the	DET
eurjchem-1701	302	3	other	other	ADJ
eurjchem-1701	302	4	hand	hand	NOUN
eurjchem-1701	302	5	,	,	PUNCT
eurjchem-1701	302	6	base	base	NOUN
eurjchem-1701	302	7	mediated	mediate	VERB
eurjchem-1701	302	8	cyclization	cyclization	NOUN
eurjchem-1701	302	9	of	of	ADP
eurjchem-1701	302	10	compound	compound	NOUN
eurjchem-1701	302	11	11	11	NUM
eurjchem-1701	302	12	afforded	afford	VERB
eurjchem-1701	302	13	triazolethione	triazolethione	NOUN
eurjchem-1701	302	14	14	14	NUM
eurjchem-1701	302	15	in	in	ADP
eurjchem-1701	302	16	93	93	NUM
eurjchem-1701	302	17	%	%	NOUN
eurjchem-1701	302	18	yield	yield	NOUN
eurjchem-1701	302	19	via	via	ADP
eurjchem-1701	302	20	thiophene	thiophene	NOUN
eurjchem-1701	302	21	intermediate	intermediate	ADJ
eurjchem-1701	302	22	(	(	PUNCT
eurjchem-1701	302	23	scheme	scheme	NOUN
eurjchem-1701	302	24	4	4	NUM
eurjchem-1701	302	25	)	)	PUNCT
eurjchem-1701	302	26	.	.	PUNCT
eurjchem-1701	303	1	the	the	DET
eurjchem-1701	303	2	thiourea	thiourea	NOUN
eurjchem-1701	303	3	derivative	derivative	NOUN
eurjchem-1701	303	4	of	of	ADP
eurjchem-1701	303	5	type	type	NOUN
eurjchem-1701	303	6	15	15	NUM
eurjchem-1701	303	7	was	be	AUX
eurjchem-1701	303	8	obtained	obtain	VERB
eurjchem-1701	303	9	in	in	ADP
eurjchem-1701	303	10	70	70	NUM
eurjchem-1701	303	11	%	%	NOUN
eurjchem-1701	303	12	yield	yield	NOUN
eurjchem-1701	303	13	as	as	ADP
eurjchem-1701	303	14	a	a	DET
eurjchem-1701	303	15	result	result	NOUN
eurjchem-1701	303	16	of	of	ADP
eurjchem-1701	303	17	addition	addition	NOUN
eurjchem-1701	303	18	of	of	ADP
eurjchem-1701	303	19	ethyl	ethyl	PROPN
eurjchem-1701	303	20	2	2	NUM
eurjchem-1701	303	21	-	-	PUNCT
eurjchem-1701	303	22	amino-4,5,6,7	amino-4,5,6,7	NOUN
eurjchem-1701	303	23	-	-	PUNCT
eurjchem-1701	303	24	tetra	tetra	NOUN
eurjchem-1701	303	25	hydrobenzo[b]thiophene-3	hydrobenzo[b]thiophene-3	NOUN
eurjchem-1701	303	26	-	-	NOUN
eurjchem-1701	303	27	carboxylate	carboxylate	NOUN
eurjchem-1701	303	28	in	in	ADP
eurjchem-1701	303	29	dioxane	dioxane	NOUN
eurjchem-1701	303	30	to	to	PART
eurjchem-1701	303	31	thienoylisothiocyante	thienoylisothiocyante	VERB
eurjchem-1701	303	32	1	1	NUM
eurjchem-1701	303	33	(	(	PUNCT
eurjchem-1701	303	34	scheme	scheme	NOUN
eurjchem-1701	303	35	5	5	NUM
eurjchem-1701	303	36	)	)	PUNCT
eurjchem-1701	303	37	.	.	PUNCT
eurjchem-1701	304	1	upon	upon	SCONJ
eurjchem-1701	304	2	heating	heating	NOUN
eurjchem-1701	304	3	of	of	ADP
eurjchem-1701	304	4	compound	compound	NOUN
eurjchem-1701	304	5	15	15	NUM
eurjchem-1701	304	6	with	with	ADP
eurjchem-1701	304	7	ethoxide	ethoxide	NOUN
eurjchem-1701	304	8	produced	produce	VERB
eurjchem-1701	304	9	thiophene-3	thiophene-3	NUM
eurjchem-1701	304	10	-	-	PUNCT
eurjchem-1701	304	11	carboxylic	carboxylic	ADJ
eurjchem-1701	304	12	acid	acid	NOUN
eurjchem-1701	304	13	16	16	NUM
eurjchem-1701	304	14	in	in	ADP
eurjchem-1701	304	15	86	86	NUM
eurjchem-1701	304	16	%	%	NOUN
eurjchem-1701	304	17	yield	yield	NOUN
eurjchem-1701	304	18	but	but	CCONJ
eurjchem-1701	304	19	the	the	DET
eurjchem-1701	304	20	other	other	ADJ
eurjchem-1701	304	21	cyclized	cyclized	ADJ
eurjchem-1701	304	22	product	product	NOUN
eurjchem-1701	304	23	17	17	NUM
eurjchem-1701	304	24	was	be	AUX
eurjchem-1701	304	25	not	not	PART
eurjchem-1701	304	26	formed	form	VERB
eurjchem-1701	304	27	.	.	PUNCT
eurjchem-1701	305	1	moreover	moreover	ADV
eurjchem-1701	305	2	,	,	PUNCT
eurjchem-1701	305	3	addition	addition	NOUN
eurjchem-1701	305	4	of	of	ADP
eurjchem-1701	305	5	amino	amino	ADJ
eurjchem-1701	305	6	phenol	phenol	NOUN
eurjchem-1701	305	7	sulfonic	sulfonic	ADJ
eurjchem-1701	305	8	acid	acid	NOUN
eurjchem-1701	305	9	derivative	derivative	NOUN
eurjchem-1701	305	10	to	to	PART
eurjchem-1701	305	11	heteroallene	heteroallene	VERB
eurjchem-1701	305	12	1	1	NUM
eurjchem-1701	305	13	in	in	ADP
eurjchem-1701	305	14	dioxane	dioxane	NOUN
eurjchem-1701	305	15	resulted	result	VERB
eurjchem-1701	305	16	in	in	ADP
eurjchem-1701	305	17	building	build	VERB
eurjchem-1701	305	18	the	the	DET
eurjchem-1701	305	19	oxazine	oxazine	NOUN
eurjchem-1701	305	20	structure	structure	NOUN
eurjchem-1701	305	21	18	18	NUM
eurjchem-1701	305	22	in	in	ADP
eurjchem-1701	305	23	65	65	NUM
eurjchem-1701	305	24	%	%	NOUN
eurjchem-1701	305	25	yield	yield	NOUN
eurjchem-1701	305	26	.	.	PUNCT
eurjchem-1701	306	1	on	on	ADP
eurjchem-1701	306	2	the	the	DET
eurjchem-1701	306	3	other	other	ADJ
eurjchem-1701	306	4	hand	hand	NOUN
eurjchem-1701	306	5	,	,	PUNCT
eurjchem-1701	306	6	nucleophilic	nucleophilic	ADJ
eurjchem-1701	306	7	addition	addition	NOUN
eurjchem-1701	306	8	of	of	ADP
eurjchem-1701	306	9	ethylene	ethylene	NOUN
eurjchem-1701	306	10	diamine	diamine	NOUN
eurjchem-1701	306	11	in	in	ADP
eurjchem-1701	306	12	dioxane	dioxane	NOUN
eurjchem-1701	306	13	to	to	ADP
eurjchem-1701	306	14	thiophene-2carbonyl	thiophene-2carbonyl	NOUN
eurjchem-1701	306	15	isothiocyanate	isothiocyanate	ADJ
eurjchem-1701	306	16	(	(	PUNCT
eurjchem-1701	306	17	1	1	NUM
eurjchem-1701	306	18	)	)	PUNCT
eurjchem-1701	306	19	led	lead	VERB
eurjchem-1701	306	20	to	to	ADP
eurjchem-1701	306	21	formation	formation	NOUN
eurjchem-1701	306	22	of	of	ADP
eurjchem-1701	306	23	imidazole	imidazole	NOUN
eurjchem-1701	306	24	derivative	derivative	NOUN
eurjchem-1701	306	25	19	19	NUM
eurjchem-1701	306	26	in	in	ADP
eurjchem-1701	306	27	74	74	NUM
eurjchem-1701	306	28	%	%	NOUN
eurjchem-1701	306	29	yield	yield	NOUN
eurjchem-1701	306	30	as	as	SCONJ
eurjchem-1701	306	31	outlined	outline	VERB
eurjchem-1701	306	32	in	in	ADP
eurjchem-1701	306	33	scheme	scheme	NOUN
eurjchem-1701	306	34	5	5	NUM
eurjchem-1701	306	35	.	.	PUNCT
eurjchem-1701	307	1	the	the	DET
eurjchem-1701	307	2	1h	1h	NUM
eurjchem-1701	307	3	nmr	nmr	NOUN
eurjchem-1701	307	4	spectrum	spectrum	NOUN
eurjchem-1701	307	5	of	of	ADP
eurjchem-1701	307	6	thiophene	thiophene	NOUN
eurjchem-1701	307	7	carboxylic	carboxylic	ADJ
eurjchem-1701	307	8	acid	acid	NOUN
eurjchem-1701	307	9	16	16	NUM
eurjchem-1701	307	10	revealed	reveal	VERB
eurjchem-1701	307	11	three	three	NUM
eurjchem-1701	307	12	sharp	sharp	ADJ
eurjchem-1701	307	13	singlets	singlet	NOUN
eurjchem-1701	307	14	at	at	ADP
eurjchem-1701	307	15	δ	δ	PROPN
eurjchem-1701	307	16	14.61	14.61	NUM
eurjchem-1701	307	17	,	,	PUNCT
eurjchem-1701	307	18	13.29	13.29	NUM
eurjchem-1701	307	19	and	and	CCONJ
eurjchem-1701	307	20	11.76	11.76	NUM
eurjchem-1701	307	21	ppm	ppm	NOUN
eurjchem-1701	307	22	for	for	ADP
eurjchem-1701	307	23	oh	oh	INTJ
eurjchem-1701	307	24	and	and	CCONJ
eurjchem-1701	307	25	2nh	2nh	ADJ
eurjchem-1701	307	26	protons	proton	NOUN
eurjchem-1701	307	27	which	which	PRON
eurjchem-1701	307	28	were	be	AUX
eurjchem-1701	307	29	d2o	d2o	NOUN
eurjchem-1701	307	30	exchangeable	exchangeable	ADJ
eurjchem-1701	307	31	.	.	PUNCT
eurjchem-1701	308	1	a	a	DET
eurjchem-1701	308	2	triplet	triplet	NOUN
eurjchem-1701	308	3	peak	peak	NOUN
eurjchem-1701	308	4	at	at	ADP
eurjchem-1701	308	5	δ	δ	PROPN
eurjchem-1701	308	6	8.29	8.29	NUM
eurjchem-1701	308	7	ppm	ppm	NOUN
eurjchem-1701	308	8	with	with	ADP
eurjchem-1701	308	9	j	j	PROPN
eurjchem-1701	308	10	=	=	SYM
eurjchem-1701	308	11	4.8	4.8	NUM
eurjchem-1701	308	12	and	and	CCONJ
eurjchem-1701	308	13	3.6	3.6	NUM
eurjchem-1701	308	14	hz	hz	NOUN
eurjchem-1701	308	15	for	for	ADP
eurjchem-1701	308	16	thiophene	thiophene	NOUN
eurjchem-1701	308	17	-	-	PUNCT
eurjchem-1701	308	18	hb	hb	NOUN
eurjchem-1701	308	19	.	.	PUNCT
eurjchem-1701	309	1	there	there	PRON
eurjchem-1701	309	2	are	be	VERB
eurjchem-1701	309	3	two	two	NUM
eurjchem-1701	309	4	doublets	doublet	NOUN
eurjchem-1701	309	5	at	at	ADP
eurjchem-1701	309	6	δ	δ	PROPN
eurjchem-1701	309	7	8.01	8.01	NUM
eurjchem-1701	309	8	and	and	CCONJ
eurjchem-1701	309	9	7.23	7.23	NUM
eurjchem-1701	309	10	ppm	ppm	NOUN
eurjchem-1701	309	11	for	for	ADP
eurjchem-1701	309	12	thiophene	thiophene	NOUN
eurjchem-1701	309	13	-	-	PUNCT
eurjchem-1701	309	14	ha	ha	INTJ
eurjchem-1701	309	15	and	and	CCONJ
eurjchem-1701	309	16	thiophene	thiophene	NOUN
eurjchem-1701	309	17	-	-	PUNCT
eurjchem-1701	309	18	hc	hc	NOUN
eurjchem-1701	309	19	.	.	NOUN
eurjchem-1701	309	20	3.2	3.2	NUM
eurjchem-1701	309	21	.	.	PUNCT
eurjchem-1701	310	1	antitumor	antitumor	PROPN
eurjchem-1701	310	2	activity	activity	NOUN
eurjchem-1701	310	3	the	the	DET
eurjchem-1701	310	4	inhibitory	inhibitory	ADJ
eurjchem-1701	310	5	activities	activity	NOUN
eurjchem-1701	310	6	of	of	ADP
eurjchem-1701	310	7	the	the	DET
eurjchem-1701	310	8	compounds	compound	NOUN
eurjchem-1701	310	9	8	8	NUM
eurjchem-1701	310	10	,	,	PUNCT
eurjchem-1701	310	11	12	12	NUM
eurjchem-1701	310	12	,	,	PUNCT
eurjchem-1701	310	13	13	13	NUM
eurjchem-1701	310	14	,	,	PUNCT
eurjchem-1701	310	15	15	15	NUM
eurjchem-1701	310	16	,	,	PUNCT
eurjchem-1701	310	17	16	16	NUM
eurjchem-1701	310	18	and	and	CCONJ
eurjchem-1701	310	19	18	18	NUM
eurjchem-1701	310	20	were	be	AUX
eurjchem-1701	310	21	evaluated	evaluate	VERB
eurjchem-1701	310	22	on	on	ADP
eurjchem-1701	310	23	the	the	DET
eurjchem-1701	310	24	in	in	X
eurjchem-1701	310	25	vitro	vitro	X
eurjchem-1701	310	26	growth	growth	NOUN
eurjchem-1701	310	27	of	of	ADP
eurjchem-1701	310	28	cancer	cancer	NOUN
eurjchem-1701	310	29	human	human	ADJ
eurjchem-1701	310	30	cell	cell	NOUN
eurjchem-1701	310	31	line	line	NOUN
eurjchem-1701	310	32	breast	breast	NOUN
eurjchem-1701	310	33	adenocarcinoma	adenocarcinoma	NOUN
eurjchem-1701	310	34	mcf-7	mcf-7	NOUN
eurjchem-1701	310	35	.	.	PUNCT
eurjchem-1701	311	1	nearly	nearly	ADV
eurjchem-1701	311	2	,	,	PUNCT
eurjchem-1701	311	3	all	all	DET
eurjchem-1701	311	4	the	the	DET
eurjchem-1701	311	5	screened	screen	VERB
eurjchem-1701	311	6	compounds	compound	NOUN
eurjchem-1701	311	7	were	be	AUX
eurjchem-1701	311	8	able	able	ADJ
eurjchem-1701	311	9	to	to	PART
eurjchem-1701	311	10	inhibit	inhibit	VERB
eurjchem-1701	311	11	the	the	DET
eurjchem-1701	311	12	growth	growth	NOUN
eurjchem-1701	311	13	of	of	ADP
eurjchem-1701	311	14	the	the	DET
eurjchem-1701	311	15	tested	test	VERB
eurjchem-1701	311	16	human	human	ADJ
eurjchem-1701	311	17	tumor	tumor	NOUN
eurjchem-1701	311	18	cell	cell	NOUN
eurjchem-1701	311	19	line	line	NOUN
eurjchem-1701	311	20	.	.	PUNCT
eurjchem-1701	312	1	the	the	DET
eurjchem-1701	312	2	results	result	NOUN
eurjchem-1701	312	3	tabulated	tabulate	VERB
eurjchem-1701	312	4	in	in	ADP
eurjchem-1701	312	5	table	table	NOUN
eurjchem-1701	312	6	1	1	NUM
eurjchem-1701	312	7	indicated	indicate	VERB
eurjchem-1701	312	8	that	that	SCONJ
eurjchem-1701	312	9	compounds	compound	VERB
eurjchem-1701	312	10	12	12	NUM
eurjchem-1701	312	11	,	,	PUNCT
eurjchem-1701	312	12	13	13	NUM
eurjchem-1701	312	13	,	,	PUNCT
eurjchem-1701	312	14	15	15	NUM
eurjchem-1701	312	15	and	and	CCONJ
eurjchem-1701	312	16	16	16	NUM
eurjchem-1701	312	17	showed	show	VERB
eurjchem-1701	312	18	the	the	DET
eurjchem-1701	312	19	highest	high	ADJ
eurjchem-1701	312	20	inhibitory	inhibitory	ADJ
eurjchem-1701	312	21	effect	effect	NOUN
eurjchem-1701	312	22	against	against	ADP
eurjchem-1701	312	23	mcf-7	mcf-7	PUNCT
eurjchem-1701	312	24	cell	cell	NOUN
eurjchem-1701	312	25	line	line	NOUN
eurjchem-1701	312	26	compared	compare	VERB
eurjchem-1701	312	27	to	to	ADP
eurjchem-1701	312	28	the	the	DET
eurjchem-1701	312	29	reference	reference	NOUN
eurjchem-1701	312	30	doxorubicin	doxorubicin	PROPN
eurjchem-1701	312	31	.	.	PUNCT
eurjchem-1701	313	1	meanwhile	meanwhile	ADV
eurjchem-1701	313	2	compounds	compound	VERB
eurjchem-1701	313	3	18	18	NUM
eurjchem-1701	313	4	and	and	CCONJ
eurjchem-1701	313	5	8	8	NUM
eurjchem-1701	313	6	exhibited	exhibit	VERB
eurjchem-1701	313	7	high	high	ADJ
eurjchem-1701	313	8	inhibitory	inhibitory	ADJ
eurjchem-1701	313	9	effects	effect	NOUN
eurjchem-1701	313	10	,	,	PUNCT
eurjchem-1701	313	11	which	which	PRON
eurjchem-1701	313	12	are	be	AUX
eurjchem-1701	313	13	less	less	ADJ
eurjchem-1701	313	14	than	than	ADP
eurjchem-1701	313	15	the	the	DET
eurjchem-1701	313	16	standard	standard	ADJ
eurjchem-1701	313	17	reference	reference	NOUN
eurjchem-1701	313	18	in	in	ADP
eurjchem-1701	313	19	table	table	NOUN
eurjchem-1701	313	20	1	1	NUM
eurjchem-1701	313	21	.	.	SYM
eurjchem-1701	313	22	2018	2018	NUM
eurjchem-1701	313	23	–	–	PUNCT
eurjchem-1701	313	24	european	european	ADJ
eurjchem-1701	313	25	journal	journal	NOUN
eurjchem-1701	313	26	of	of	ADP
eurjchem-1701	313	27	chemistry	chemistry	NOUN
eurjchem-1701	313	28	–	–	PUNCT
eurjchem-1701	313	29	cc	cc	NOUN
eurjchem-1701	313	30	by	by	ADP
eurjchem-1701	313	31	nc	nc	PROPN
eurjchem-1701	313	32	–	–	PUNCT
eurjchem-1701	313	33	doi	doi	NOUN
eurjchem-1701	313	34	:	:	PUNCT
eurjchem-1701	313	35	10.5155	10.5155	NUM
eurjchem-1701	313	36	/	/	SYM
eurjchem-1701	313	37	eurjchem.9.2.99	eurjchem.9.2.99	NUM
eurjchem-1701	313	38	-	-	PUNCT
eurjchem-1701	313	39	106.1701	106.1701	NUM
eurjchem-1701	313	40	106	106	NUM
eurjchem-1701	313	41	haggam	haggam	NOUN
eurjchem-1701	313	42	et	et	PROPN
eurjchem-1701	313	43	al	al	PROPN
eurjchem-1701	313	44	.	.	PUNCT
eurjchem-1701	313	45	/	/	SYM
eurjchem-1701	313	46	european	european	PROPN
eurjchem-1701	313	47	journal	journal	PROPN
eurjchem-1701	313	48	of	of	ADP
eurjchem-1701	313	49	chemistry	chemistry	NOUN
eurjchem-1701	313	50	9	9	NUM
eurjchem-1701	313	51	(	(	PUNCT
eurjchem-1701	313	52	2	2	NUM
eurjchem-1701	313	53	)	)	PUNCT
eurjchem-1701	313	54	(	(	PUNCT
eurjchem-1701	313	55	2018	2018	NUM
eurjchem-1701	313	56	)	)	PUNCT
eurjchem-1701	313	57	99	99	NUM
eurjchem-1701	313	58	-	-	SYM
eurjchem-1701	313	59	106	106	NUM
eurjchem-1701	313	60	the	the	DET
eurjchem-1701	313	61	cytotoxic	cytotoxic	ADJ
eurjchem-1701	313	62	and	and	CCONJ
eurjchem-1701	313	63	antitumor	antitumor	PROPN
eurjchem-1701	313	64	activities	activity	NOUN
eurjchem-1701	313	65	of	of	ADP
eurjchem-1701	313	66	the	the	DET
eurjchem-1701	313	67	compounds	compound	NOUN
eurjchem-1701	313	68	8	8	NUM
eurjchem-1701	313	69	,	,	PUNCT
eurjchem-1701	313	70	12	12	NUM
eurjchem-1701	313	71	,	,	PUNCT
eurjchem-1701	313	72	13	13	NUM
eurjchem-1701	313	73	,	,	PUNCT
eurjchem-1701	313	74	15	15	NUM
eurjchem-1701	313	75	,	,	PUNCT
eurjchem-1701	313	76	16	16	NUM
eurjchem-1701	313	77	and	and	CCONJ
eurjchem-1701	313	78	18	18	NUM
eurjchem-1701	313	79	were	be	AUX
eurjchem-1701	313	80	tested	test	VERB
eurjchem-1701	313	81	against	against	ADP
eurjchem-1701	313	82	mcf-7	mcf-7	NOUN
eurjchem-1701	313	83	cells	cell	NOUN
eurjchem-1701	313	84	line	line	NOUN
eurjchem-1701	313	85	.	.	PUNCT
eurjchem-1701	314	1	the	the	DET
eurjchem-1701	314	2	inhibitory	inhibitory	ADJ
eurjchem-1701	314	3	activities	activity	NOUN
eurjchem-1701	314	4	were	be	AUX
eurjchem-1701	314	5	detected	detect	VERB
eurjchem-1701	314	6	by	by	ADP
eurjchem-1701	314	7	using	use	VERB
eurjchem-1701	314	8	different	different	ADJ
eurjchem-1701	314	9	concentrations	concentration	NOUN
eurjchem-1701	314	10	as	as	SCONJ
eurjchem-1701	314	11	shown	show	VERB
eurjchem-1701	314	12	in	in	ADP
eurjchem-1701	314	13	table	table	NOUN
eurjchem-1701	314	14	2	2	NUM
eurjchem-1701	314	15	.	.	PUNCT
eurjchem-1701	314	16	results	result	NOUN
eurjchem-1701	314	17	presented	present	VERB
eurjchem-1701	314	18	in	in	ADP
eurjchem-1701	314	19	table	table	NOUN
eurjchem-1701	314	20	2	2	NUM
eurjchem-1701	314	21	displayed	display	VERB
eurjchem-1701	314	22	that	that	SCONJ
eurjchem-1701	314	23	,	,	PUNCT
eurjchem-1701	314	24	compounds	compound	VERB
eurjchem-1701	314	25	15	15	NUM
eurjchem-1701	314	26	,	,	PUNCT
eurjchem-1701	314	27	16	16	NUM
eurjchem-1701	314	28	,	,	PUNCT
eurjchem-1701	314	29	13	13	NUM
eurjchem-1701	314	30	and	and	CCONJ
eurjchem-1701	314	31	12	12	NUM
eurjchem-1701	314	32	had	have	VERB
eurjchem-1701	314	33	very	very	ADV
eurjchem-1701	314	34	strong	strong	ADJ
eurjchem-1701	314	35	cytotoxic	cytotoxic	ADJ
eurjchem-1701	314	36	antitumor	antitumor	NOUN
eurjchem-1701	314	37	activity	activity	NOUN
eurjchem-1701	314	38	,	,	PUNCT
eurjchem-1701	314	39	while	while	SCONJ
eurjchem-1701	314	40	compounds	compound	NOUN
eurjchem-1701	314	41	18	18	NUM
eurjchem-1701	314	42	and	and	CCONJ
eurjchem-1701	314	43	8	8	NUM
eurjchem-1701	314	44	have	have	VERB
eurjchem-1701	314	45	strong	strong	ADJ
eurjchem-1701	314	46	cytotoxic	cytotoxic	ADJ
eurjchem-1701	314	47	antitumor	antitumor	NOUN
eurjchem-1701	314	48	activity	activity	NOUN
eurjchem-1701	314	49	against	against	ADP
eurjchem-1701	314	50	mcf-7	mcf-7	NOUN
eurjchem-1701	314	51	cell	cell	NOUN
eurjchem-1701	314	52	line	line	NOUN
eurjchem-1701	314	53	.	.	PUNCT
eurjchem-1701	315	1	4	4	X
eurjchem-1701	315	2	.	.	X
eurjchem-1701	315	3	conclusion	conclusion	NOUN
eurjchem-1701	315	4	in	in	ADP
eurjchem-1701	315	5	conclusion	conclusion	NOUN
eurjchem-1701	315	6	,	,	PUNCT
eurjchem-1701	315	7	we	we	PRON
eurjchem-1701	315	8	were	be	AUX
eurjchem-1701	315	9	able	able	ADJ
eurjchem-1701	315	10	to	to	PART
eurjchem-1701	315	11	realize	realize	VERB
eurjchem-1701	315	12	the	the	DET
eurjchem-1701	315	13	synthesis	synthesis	NOUN
eurjchem-1701	315	14	of	of	ADP
eurjchem-1701	315	15	a	a	DET
eurjchem-1701	315	16	series	series	NOUN
eurjchem-1701	315	17	of	of	ADP
eurjchem-1701	315	18	new	new	ADJ
eurjchem-1701	315	19	1,2,4	1,2,4	NUM
eurjchem-1701	315	20	-	-	PUNCT
eurjchem-1701	315	21	triazolethione	triazolethione	NOUN
eurjchem-1701	315	22	,	,	PUNCT
eurjchem-1701	315	23	1,3,4	1,3,4	NUM
eurjchem-1701	315	24	-	-	PUNCT
eurjchem-1701	315	25	thiadiazole	thiadiazole	NOUN
eurjchem-1701	315	26	,	,	PUNCT
eurjchem-1701	315	27	1,3imidazole	1,3imidazole	NUM
eurjchem-1701	315	28	and	and	CCONJ
eurjchem-1701	315	29	oxadiazine	oxadiazine	NOUN
eurjchem-1701	315	30	derivatives	derivative	NOUN
eurjchem-1701	315	31	bearing	bear	VERB
eurjchem-1701	315	32	thiophene	thiophene	NOUN
eurjchem-1701	315	33	ring	ring	NOUN
eurjchem-1701	315	34	system	system	NOUN
eurjchem-1701	315	35	in	in	ADP
eurjchem-1701	315	36	high	high	ADJ
eurjchem-1701	315	37	yields	yield	NOUN
eurjchem-1701	315	38	61	61	NUM
eurjchem-1701	315	39	-	-	SYM
eurjchem-1701	315	40	95	95	NUM
eurjchem-1701	315	41	%	%	NOUN
eurjchem-1701	315	42	.	.	PUNCT
eurjchem-1701	316	1	compounds	compound	NOUN
eurjchem-1701	316	2	were	be	AUX
eurjchem-1701	316	3	screened	screen	VERB
eurjchem-1701	316	4	for	for	ADP
eurjchem-1701	316	5	their	their	PRON
eurjchem-1701	316	6	anticancer	anticancer	NOUN
eurjchem-1701	316	7	activity	activity	NOUN
eurjchem-1701	316	8	on	on	ADP
eurjchem-1701	316	9	cancer	cancer	NOUN
eurjchem-1701	316	10	human	human	ADJ
eurjchem-1701	316	11	cell	cell	NOUN
eurjchem-1701	316	12	lines	line	NOUN
eurjchem-1701	316	13	like	like	ADP
eurjchem-1701	316	14	breast	breast	NOUN
eurjchem-1701	316	15	cancer	cancer	NOUN
eurjchem-1701	316	16	mcf-7	mcf-7	PUNCT
eurjchem-1701	316	17	.	.	PUNCT
eurjchem-1701	317	1	most	most	ADJ
eurjchem-1701	317	2	of	of	ADP
eurjchem-1701	317	3	selected	select	VERB
eurjchem-1701	317	4	compounds	compound	NOUN
eurjchem-1701	317	5	showed	show	VERB
eurjchem-1701	317	6	remarkable	remarkable	ADJ
eurjchem-1701	317	7	antitumor	antitumor	PROPN
eurjchem-1701	317	8	activity	activity	NOUN
eurjchem-1701	317	9	.	.	PUNCT
eurjchem-1701	318	1	compounds	compound	VERB
eurjchem-1701	318	2	12	12	NUM
eurjchem-1701	318	3	,	,	PUNCT
eurjchem-1701	318	4	13	13	NUM
eurjchem-1701	318	5	,	,	PUNCT
eurjchem-1701	318	6	15	15	NUM
eurjchem-1701	318	7	and	and	CCONJ
eurjchem-1701	318	8	16	16	NUM
eurjchem-1701	318	9	are	be	AUX
eurjchem-1701	318	10	the	the	DET
eurjchem-1701	318	11	most	most	ADV
eurjchem-1701	318	12	active	active	ADJ
eurjchem-1701	318	13	ones	one	NOUN
eurjchem-1701	318	14	on	on	ADP
eurjchem-1701	318	15	the	the	DET
eurjchem-1701	318	16	cancer	cancer	NOUN
eurjchem-1701	318	17	cell	cell	NOUN
eurjchem-1701	318	18	line	line	NOUN
eurjchem-1701	318	19	due	due	ADP
eurjchem-1701	318	20	to	to	ADP
eurjchem-1701	318	21	their	their	PRON
eurjchem-1701	318	22	reactivity	reactivity	NOUN
eurjchem-1701	318	23	is	be	AUX
eurjchem-1701	318	24	more	more	ADJ
eurjchem-1701	318	25	than	than	ADP
eurjchem-1701	318	26	that	that	PRON
eurjchem-1701	318	27	of	of	ADP
eurjchem-1701	318	28	the	the	DET
eurjchem-1701	318	29	standard	standard	NOUN
eurjchem-1701	318	30	doxorubicin	doxorubicin	PROPN
eurjchem-1701	318	31	on	on	ADP
eurjchem-1701	318	32	the	the	DET
eurjchem-1701	318	33	same	same	ADJ
eurjchem-1701	318	34	cell	cell	NOUN
eurjchem-1701	318	35	line	line	NOUN
eurjchem-1701	318	36	.	.	PUNCT
eurjchem-1701	319	1	accordingly	accordingly	ADV
eurjchem-1701	319	2	,	,	PUNCT
eurjchem-1701	319	3	these	these	DET
eurjchem-1701	319	4	preliminary	preliminary	ADJ
eurjchem-1701	319	5	results	result	NOUN
eurjchem-1701	319	6	of	of	ADP
eurjchem-1701	319	7	the	the	DET
eurjchem-1701	319	8	newly	newly	ADV
eurjchem-1701	319	9	synthesized	synthesize	VERB
eurjchem-1701	319	10	thiophene	thiophene	NOUN
eurjchem-1701	319	11	derivatives	derivative	NOUN
eurjchem-1701	319	12	can	can	AUX
eurjchem-1701	319	13	serve	serve	VERB
eurjchem-1701	319	14	as	as	ADP
eurjchem-1701	319	15	a	a	DET
eurjchem-1701	319	16	starting	starting	NOUN
eurjchem-1701	319	17	point	point	NOUN
eurjchem-1701	319	18	for	for	ADP
eurjchem-1701	319	19	the	the	DET
eurjchem-1701	319	20	development	development	NOUN
eurjchem-1701	319	21	of	of	ADP
eurjchem-1701	319	22	potent	potent	ADJ
eurjchem-1701	319	23	anti	anti	ADJ
eurjchem-1701	319	24	-	-	ADJ
eurjchem-1701	319	25	cancer	cancer	ADJ
eurjchem-1701	319	26	agents	agent	NOUN
eurjchem-1701	319	27	.	.	PUNCT
eurjchem-1701	320	1	disclosure	disclosure	NOUN
eurjchem-1701	320	2	statement	statement	NOUN
eurjchem-1701	320	3	conflict	conflict	NOUN
eurjchem-1701	320	4	of	of	ADP
eurjchem-1701	320	5	interests	interest	NOUN
eurjchem-1701	320	6	:	:	PUNCT
eurjchem-1701	320	7	the	the	DET
eurjchem-1701	320	8	authors	author	NOUN
eurjchem-1701	320	9	declare	declare	VERB
eurjchem-1701	320	10	that	that	SCONJ
eurjchem-1701	320	11	they	they	PRON
eurjchem-1701	320	12	have	have	VERB
eurjchem-1701	320	13	no	no	DET
eurjchem-1701	320	14	conflict	conflict	NOUN
eurjchem-1701	320	15	of	of	ADP
eurjchem-1701	320	16	interest	interest	NOUN
eurjchem-1701	320	17	.	.	PUNCT
eurjchem-1701	321	1	author	author	NOUN
eurjchem-1701	321	2	contributions	contribution	NOUN
eurjchem-1701	321	3	:	:	PUNCT
eurjchem-1701	321	4	all	all	DET
eurjchem-1701	321	5	authors	author	NOUN
eurjchem-1701	321	6	contributed	contribute	VERB
eurjchem-1701	321	7	equally	equally	ADV
eurjchem-1701	321	8	to	to	ADP
eurjchem-1701	321	9	this	this	DET
eurjchem-1701	321	10	work	work	NOUN
eurjchem-1701	321	11	.	.	PUNCT
eurjchem-1701	322	1	ethical	ethical	ADJ
eurjchem-1701	322	2	approval	approval	NOUN
eurjchem-1701	322	3	:	:	PUNCT
eurjchem-1701	323	1	all	all	DET
eurjchem-1701	323	2	ethical	ethical	ADJ
eurjchem-1701	323	3	guidelines	guideline	NOUN
eurjchem-1701	323	4	have	have	AUX
eurjchem-1701	323	5	been	be	AUX
eurjchem-1701	323	6	adhered	adhere	VERB
eurjchem-1701	323	7	.	.	PUNCT
eurjchem-1701	324	1	sample	sample	NOUN
eurjchem-1701	324	2	availability	availability	NOUN
eurjchem-1701	324	3	:	:	PUNCT
eurjchem-1701	324	4	samples	sample	NOUN
eurjchem-1701	324	5	of	of	ADP
eurjchem-1701	324	6	the	the	DET
eurjchem-1701	324	7	compounds	compound	NOUN
eurjchem-1701	324	8	are	be	AUX
eurjchem-1701	324	9	available	available	ADJ
eurjchem-1701	324	10	from	from	ADP
eurjchem-1701	324	11	the	the	DET
eurjchem-1701	324	12	author	author	NOUN
eurjchem-1701	324	13	.	.	PUNCT
eurjchem-1701	325	1	orcid	orcid	PROPN
eurjchem-1701	325	2	reda	reda	PROPN
eurjchem-1701	325	3	ahmed	ahme	VERB
eurjchem-1701	325	4	haggam	haggam	PROPN
eurjchem-1701	325	5	http://orcid.org/0000-0001-8568-9668	http://orcid.org/0000-0001-8568-9668	PROPN
eurjchem-1701	325	6	references	reference	NOUN
eurjchem-1701	325	7	[	[	X
eurjchem-1701	325	8	1	1	NUM
eurjchem-1701	325	9	]	]	PUNCT
eurjchem-1701	325	10	.	.	PUNCT
eurjchem-1701	326	1	barbuceanu	barbuceanu	PROPN
eurjchem-1701	326	2	,	,	PUNCT
eurjchem-1701	326	3	s.	s.	PROPN
eurjchem-1701	326	4	f.	f.	PROPN
eurjchem-1701	326	5	;	;	PUNCT
eurjchem-1701	326	6	saramet	saramet	PROPN
eurjchem-1701	326	7	,	,	PUNCT
eurjchem-1701	326	8	g.	g.	PROPN
eurjchem-1701	326	9	;	;	PUNCT
eurjchem-1701	326	10	almajan	almajan	PROPN
eurjchem-1701	326	11	,	,	PUNCT
eurjchem-1701	326	12	g.	g.	PROPN
eurjchem-1701	326	13	l.	l.	PROPN
eurjchem-1701	326	14	;	;	PUNCT
eurjchem-1701	326	15	draghici	draghici	PROPN
eurjchem-1701	326	16	,	,	PUNCT
eurjchem-1701	326	17	c.	c.	PROPN
eurjchem-1701	326	18	;	;	PUNCT
eurjchem-1701	326	19	barbuceanu	barbuceanu	PROPN
eurjchem-1701	326	20	,	,	PUNCT
eurjchem-1701	326	21	f.	f.	PROPN
eurjchem-1701	326	22	;	;	PUNCT
eurjchem-1701	326	23	bancescu	bancescu	PROPN
eurjchem-1701	326	24	,	,	PUNCT
eurjchem-1701	326	25	g.	g.	PROPN
eurjchem-1701	326	26	bioorg	bioorg	PROPN
eurjchem-1701	326	27	.	.	PUNCT
eurjchem-1701	327	1	med	med	PROPN
eurjchem-1701	327	2	.	.	PROPN
eurjchem-1701	327	3	chem	chem	PROPN
eurjchem-1701	327	4	.	.	PUNCT
eurjchem-1701	328	1	2012	2012	NUM
eurjchem-1701	328	2	,	,	PUNCT
eurjchem-1701	328	3	49	49	NUM
eurjchem-1701	328	4	,	,	PUNCT
eurjchem-1701	328	5	417	417	NUM
eurjchem-1701	328	6	-	-	SYM
eurjchem-1701	328	7	423	423	NUM
eurjchem-1701	328	8	.	.	PUNCT
eurjchem-1701	329	1	[	[	X
eurjchem-1701	329	2	2	2	NUM
eurjchem-1701	329	3	]	]	PUNCT
eurjchem-1701	329	4	.	.	PUNCT
eurjchem-1701	329	5	sharma	sharma	PROPN
eurjchem-1701	329	6	,	,	PUNCT
eurjchem-1701	329	7	r.	r.	PROPN
eurjchem-1701	329	8	;	;	PUNCT
eurjchem-1701	329	9	misra	misra	NOUN
eurjchem-1701	329	10	,	,	PUNCT
eurjchem-1701	329	11	g.	g.	PROPN
eurjchem-1701	329	12	p.	p.	PROPN
eurjchem-1701	329	13	;	;	PUNCT
eurjchem-1701	329	14	sainy	sainy	PROPN
eurjchem-1701	329	15	,	,	PUNCT
eurjchem-1701	329	16	j.	j.	PROPN
eurjchem-1701	329	17	;	;	PUNCT
eurjchem-1701	329	18	chaturvedi	chaturvedi	PROPN
eurjchem-1701	329	19	,	,	PUNCT
eurjchem-1701	329	20	s.	s.	PROPN
eurjchem-1701	329	21	c.	c.	PROPN
eurjchem-1701	329	22	med	med	PROPN
eurjchem-1701	329	23	.	.	PUNCT
eurjchem-1701	329	24	chem	chem	PROPN
eurjchem-1701	329	25	.	.	PUNCT
eurjchem-1701	330	1	res	re	NOUN
eurjchem-1701	330	2	.	.	PROPN
eurjchem-1701	331	1	2011	2011	NUM
eurjchem-1701	331	2	,	,	PUNCT
eurjchem-1701	331	3	20	20	NUM
eurjchem-1701	331	4	,	,	PUNCT
eurjchem-1701	331	5	245	245	NUM
eurjchem-1701	331	6	-	-	SYM
eurjchem-1701	331	7	253	253	NUM
eurjchem-1701	331	8	.	.	PUNCT
eurjchem-1701	332	1	[	[	X
eurjchem-1701	332	2	3	3	NUM
eurjchem-1701	332	3	]	]	PUNCT
eurjchem-1701	332	4	.	.	PUNCT
eurjchem-1701	333	1	khan	khan	PROPN
eurjchem-1701	333	2	,	,	PUNCT
eurjchem-1701	333	3	i.	i.	PROPN
eurjchem-1701	333	4	;	;	PUNCT
eurjchem-1701	333	5	ali	ali	PROPN
eurjchem-1701	333	6	,	,	PUNCT
eurjchem-1701	333	7	s.	s.	PROPN
eurjchem-1701	333	8	;	;	PUNCT
eurjchem-1701	333	9	hameed	hameed	PROPN
eurjchem-1701	333	10	,	,	PUNCT
eurjchem-1701	333	11	s.	s.	PROPN
eurjchem-1701	333	12	;	;	PUNCT
eurjchem-1701	333	13	rama	rama	PROPN
eurjchem-1701	333	14	,	,	PUNCT
eurjchem-1701	333	15	n.	n.	PROPN
eurjchem-1701	333	16	h.	h.	PROPN
eurjchem-1701	333	17	;	;	PUNCT
eurjchem-1701	333	18	hussain	hussain	PROPN
eurjchem-1701	333	19	,	,	PUNCT
eurjchem-1701	333	20	m.	m.	NOUN
eurjchem-1701	333	21	t.	t.	PROPN
eurjchem-1701	333	22	;	;	PUNCT
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eurjchem-1701	336	4	.	.	PUNCT
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eurjchem-1701	340	4	.	.	PUNCT
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eurjchem-1701	364	8	s.	s.	PROPN
eurjchem-1701	364	9	;	;	PUNCT
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eurjchem-1701	364	11	,	,	PUNCT
eurjchem-1701	364	12	b.	b.	PROPN
eurjchem-1701	364	13	;	;	PUNCT
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eurjchem-1701	364	16	k.	k.	PROPN
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eurjchem-1701	364	22	;	;	PUNCT
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eurjchem-1701	364	30	k.	k.	PROPN
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eurjchem-1701	365	5	.	.	PUNCT
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eurjchem-1701	366	4	,	,	PUNCT
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eurjchem-1701	366	6	-	-	SYM
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eurjchem-1701	366	8	.	.	PUNCT
eurjchem-1701	367	1	[	[	X
eurjchem-1701	367	2	13	13	NUM
eurjchem-1701	367	3	]	]	PUNCT
eurjchem-1701	367	4	.	.	PUNCT
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eurjchem-1701	370	2	,	,	PUNCT
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eurjchem-1701	371	2	14	14	NUM
eurjchem-1701	371	3	]	]	PUNCT
eurjchem-1701	371	4	.	.	PUNCT
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eurjchem-1701	372	2	,	,	PUNCT
eurjchem-1701	372	3	s.	s.	PROPN
eurjchem-1701	372	4	;	;	PUNCT
eurjchem-1701	372	5	singh	singh	PROPN
eurjchem-1701	372	6	,	,	PUNCT
eurjchem-1701	372	7	b.	b.	PROPN
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eurjchem-1701	373	1	j.	j.	PROPN
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eurjchem-1701	375	1	[	[	X
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eurjchem-1701	375	3	]	]	SYM
eurjchem-1701	375	4	.	.	PUNCT
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eurjchem-1701	376	1	(	(	PUNCT
eurjchem-1701	376	2	bucharest	buchar	ADJ
eurjchem-1701	376	3	)	)	PUNCT
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eurjchem-1701	376	5	,	,	PUNCT
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eurjchem-1701	376	7	,	,	PUNCT
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eurjchem-1701	377	1	[	[	X
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eurjchem-1701	377	3	]	]	PUNCT
eurjchem-1701	377	4	.	.	PUNCT
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eurjchem-1701	378	5	;	;	PUNCT
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eurjchem-1701	378	10	;	;	PUNCT
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eurjchem-1701	378	12	,	,	PUNCT
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eurjchem-1701	379	3	.	.	PUNCT
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eurjchem-1701	380	2	,	,	PUNCT
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eurjchem-1701	380	6	-	-	SYM
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eurjchem-1701	380	8	.	.	PUNCT
eurjchem-1701	381	1	[	[	X
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eurjchem-1701	381	3	]	]	SYM
eurjchem-1701	381	4	.	.	PUNCT
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eurjchem-1701	382	5	;	;	PUNCT
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eurjchem-1701	382	10	;	;	PUNCT
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eurjchem-1701	382	13	m.	m.	PROPN
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eurjchem-1701	382	15	;	;	PUNCT
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eurjchem-1701	382	20	s.	s.	PROPN
eurjchem-1701	382	21	h.	h.	PROPN
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eurjchem-1701	382	23	.	.	PUNCT
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eurjchem-1701	383	2	.	.	PUNCT
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eurjchem-1701	384	8	-	-	SYM
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eurjchem-1701	385	1	[	[	X
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eurjchem-1701	385	3	]	]	PUNCT
eurjchem-1701	385	4	.	.	PUNCT
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eurjchem-1701	386	5	;	;	PUNCT
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eurjchem-1701	387	1	[	[	X
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eurjchem-1701	387	4	.	.	PUNCT
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eurjchem-1701	403	6	-	-	SYM
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eurjchem-1701	403	8	.	.	PUNCT
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eurjchem-1701	405	36	s.	s.	PROPN
eurjchem-1701	405	37	;	;	PUNCT
eurjchem-1701	405	38	boyd	boyd	PROPN
eurjchem-1701	405	39	,	,	PUNCT
eurjchem-1701	405	40	m.	m.	PROPN
eurjchem-1701	405	41	r.	r.	PROPN
eurjchem-1701	405	42	j.	j.	PROPN
eurjchem-1701	405	43	natl	natl	PROPN
eurjchem-1701	405	44	.	.	PUNCT
eurjchem-1701	406	1	cancer	cancer	PROPN
eurjchem-1701	406	2	inst	inst	PROPN
eurjchem-1701	406	3	.	.	PUNCT
eurjchem-1701	407	1	1990	1990	NUM
eurjchem-1701	407	2	,	,	PUNCT
eurjchem-1701	407	3	82	82	NUM
eurjchem-1701	407	4	,	,	PUNCT
eurjchem-1701	407	5	1107	1107	NUM
eurjchem-1701	407	6	-	-	SYM
eurjchem-1701	407	7	1112	1112	NUM
eurjchem-1701	407	8	.	.	PUNCT
eurjchem-1701	408	1	[	[	X
eurjchem-1701	408	2	24	24	NUM
eurjchem-1701	408	3	]	]	PUNCT
eurjchem-1701	408	4	.	.	PUNCT
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eurjchem-1701	409	2	,	,	PUNCT
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eurjchem-1701	409	4	;	;	PUNCT
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eurjchem-1701	409	6	,	,	PUNCT
eurjchem-1701	409	7	d.	d.	PROPN
eurjchem-1701	409	8	;	;	PUNCT
eurjchem-1701	409	9	skehan	skehan	PROPN
eurjchem-1701	409	10	,	,	PUNCT
eurjchem-1701	409	11	p.	p.	NOUN
eurjchem-1701	409	12	;	;	PUNCT
eurjchem-1701	409	13	shoemaker	shoemaker	PROPN
eurjchem-1701	409	14	,	,	PUNCT
eurjchem-1701	409	15	r.	r.	PROPN
eurjchem-1701	409	16	;	;	PUNCT
eurjchem-1701	409	17	paull	paull	PROPN
eurjchem-1701	409	18	,	,	PUNCT
eurjchem-1701	409	19	k.	k.	PROPN
eurjchem-1701	409	20	;	;	PUNCT
eurjchem-1701	409	21	vistica	vistica	PROPN
eurjchem-1701	409	22	,	,	PUNCT
eurjchem-1701	409	23	d.	d.	PROPN
eurjchem-1701	409	24	;	;	PUNCT
eurjchem-1701	409	25	hose	hose	PROPN
eurjchem-1701	409	26	,	,	PUNCT
eurjchem-1701	409	27	c.	c.	PROPN
eurjchem-1701	409	28	;	;	PUNCT
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eurjchem-1701	409	30	,	,	PUNCT
eurjchem-1701	409	31	j.	j.	PROPN
eurjchem-1701	409	32	;	;	PUNCT
eurjchem-1701	409	33	cronise	cronise	PROPN
eurjchem-1701	409	34	,	,	PUNCT
eurjchem-1701	409	35	p.	p.	NOUN
eurjchem-1701	409	36	;	;	PUNCT
eurjchem-1701	409	37	vaigro	vaigro	NOUN
eurjchem-1701	409	38	-	-	PUNCT
eurjchem-1701	409	39	wolff	wolff	NOUN
eurjchem-1701	409	40	,	,	PUNCT
eurjchem-1701	409	41	a.	a.	NOUN
eurjchem-1701	409	42	;	;	PUNCT
eurjchem-1701	409	43	gray	gray	ADJ
eurjchem-1701	409	44	-	-	PUNCT
eurjchem-1701	409	45	goodrich	goodrich	NOUN
eurjchem-1701	409	46	,	,	PUNCT
eurjchem-1701	409	47	m.	m.	NOUN
eurjchem-1701	409	48	;	;	PUNCT
eurjchem-1701	409	49	campbell	campbell	PROPN
eurjchem-1701	409	50	,	,	PUNCT
eurjchem-1701	409	51	h.	h.	PROPN
eurjchem-1701	409	52	;	;	PUNCT
eurjchem-1701	409	53	mayo	mayo	PROPN
eurjchem-1701	409	54	,	,	PUNCT
eurjchem-1701	409	55	j.	j.	PROPN
eurjchem-1701	409	56	;	;	PUNCT
eurjchem-1701	409	57	boyd	boyd	PROPN
eurjchem-1701	409	58	,	,	PUNCT
eurjchem-1701	409	59	m.	m.	PROPN
eurjchem-1701	409	60	j.	j.	PROPN
eurjchem-1701	409	61	natl	natl	PROPN
eurjchem-1701	409	62	.	.	PUNCT
eurjchem-1701	410	1	cancer	cancer	PROPN
eurjchem-1701	410	2	inst	inst	PROPN
eurjchem-1701	410	3	.	.	PROPN
eurjchem-1701	410	4	1991	1991	NUM
eurjchem-1701	410	5	,	,	PUNCT
eurjchem-1701	410	6	83	83	NUM
eurjchem-1701	410	7	,	,	PUNCT
eurjchem-1701	410	8	757766	757766	NUM
eurjchem-1701	410	9	.	.	PUNCT
eurjchem-1701	411	1	[	[	X
eurjchem-1701	411	2	25	25	NUM
eurjchem-1701	411	3	]	]	PUNCT
eurjchem-1701	411	4	.	.	PUNCT
eurjchem-1701	412	1	kibrom	kibrom	PROPN
eurjchem-1701	412	2	,	,	PUNCT
eurjchem-1701	412	3	g.	g.	PROPN
eurjchem-1701	412	4	b.	b.	PROPN
eurjchem-1701	412	5	;	;	PUNCT
eurjchem-1701	412	6	girija	girija	PROPN
eurjchem-1701	412	7	,	,	PUNCT
eurjchem-1701	412	8	s.	s.	PROPN
eurjchem-1701	412	9	s.	s.	PROPN
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eurjchem-1701	412	11	2015	2015	NUM
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eurjchem-1701	412	13	6	6	NUM
eurjchem-1701	412	14	,	,	PUNCT
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eurjchem-1701	412	16	-	-	SYM
eurjchem-1701	412	17	213	213	NUM
eurjchem-1701	412	18	.	.	PUNCT
eurjchem-1701	413	1	[	[	X
eurjchem-1701	413	2	26	26	NUM
eurjchem-1701	413	3	]	]	PUNCT
eurjchem-1701	413	4	.	.	PUNCT
eurjchem-1701	414	1	mukerjee	mukerjee	PROPN
eurjchem-1701	414	2	,	,	PUNCT
eurjchem-1701	414	3	a.	a.	PROPN
eurjchem-1701	414	4	k.	k.	PROPN
eurjchem-1701	414	5	;	;	PUNCT
eurjchem-1701	414	6	ashare	ashare	PROPN
eurjchem-1701	414	7	,	,	PUNCT
eurjchem-1701	414	8	r.	r.	PROPN
eurjchem-1701	414	9	chem	chem	PROPN
eurjchem-1701	414	10	.	.	PUNCT
eurjchem-1701	415	1	rev	rev	PROPN
eurjchem-1701	415	2	.	.	PROPN
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eurjchem-1701	415	4	,	,	PUNCT
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eurjchem-1701	415	6	,	,	PUNCT
eurjchem-1701	415	7	1	1	NUM
eurjchem-1701	415	8	-	-	SYM
eurjchem-1701	415	9	24	24	NUM
eurjchem-1701	415	10	.	.	PUNCT
eurjchem-1701	416	1	[	[	X
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eurjchem-1701	416	3	]	]	PUNCT
eurjchem-1701	416	4	.	.	PUNCT
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eurjchem-1701	417	4	,	,	PUNCT
eurjchem-1701	417	5	s.	s.	PROPN
eurjchem-1701	417	6	;	;	PUNCT
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eurjchem-1701	417	8	,	,	PUNCT
eurjchem-1701	417	9	m.	m.	NOUN
eurjchem-1701	417	10	g.	g.	PROPN
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eurjchem-1701	417	13	,	,	PUNCT
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eurjchem-1701	417	16	.	.	PUNCT
eurjchem-1701	418	1	czech	czech	PROPN
eurjchem-1701	418	2	.	.	PUNCT
eurjchem-1701	419	1	chem	chem	PROPN
eurjchem-1701	419	2	.	.	PUNCT
eurjchem-1701	420	1	commun	commun	PROPN
eurjchem-1701	420	2	.	.	PUNCT
eurjchem-1701	421	1	1990	1990	NUM
eurjchem-1701	421	2	,	,	PUNCT
eurjchem-1701	421	3	55	55	NUM
eurjchem-1701	421	4	,	,	PUNCT
eurjchem-1701	421	5	1049	1049	NUM
eurjchem-1701	421	6	-	-	SYM
eurjchem-1701	421	7	1054	1054	NUM
eurjchem-1701	421	8	.	.	PUNCT
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eurjchem-1701	422	2	©	©	PROPN
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eurjchem-1701	422	6	.	.	PUNCT
eurjchem-1701	423	1	this	this	DET
eurjchem-1701	423	2	work	work	NOUN
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eurjchem-1701	423	4	published	publish	VERB
eurjchem-1701	423	5	and	and	CCONJ
eurjchem-1701	423	6	licensed	license	VERB
eurjchem-1701	423	7	by	by	ADP
eurjchem-1701	423	8	atlanta	atlanta	PROPN
eurjchem-1701	423	9	publishing	publishing	PROPN
eurjchem-1701	423	10	house	house	PROPN
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eurjchem-1701	423	13	atlanta	atlanta	PROPN
eurjchem-1701	423	14	,	,	PUNCT
eurjchem-1701	423	15	ga	ga	PROPN
eurjchem-1701	423	16	,	,	PUNCT
eurjchem-1701	423	17	usa	usa	PROPN
eurjchem-1701	423	18	.	.	PUNCT
eurjchem-1701	424	1	the	the	DET
eurjchem-1701	424	2	full	full	ADJ
eurjchem-1701	424	3	terms	term	NOUN
eurjchem-1701	424	4	of	of	ADP
eurjchem-1701	424	5	this	this	DET
eurjchem-1701	424	6	license	license	NOUN
eurjchem-1701	424	7	are	be	AUX
eurjchem-1701	424	8	available	available	ADJ
eurjchem-1701	424	9	at	at	ADP
eurjchem-1701	424	10	http://www.eurjchem.com/index.php/eurjchem/pages/view/terms	http://www.eurjchem.com/index.php/eurjchem/pages/view/term	NOUN
eurjchem-1701	424	11	and	and	CCONJ
eurjchem-1701	424	12	incorporate	incorporate	VERB
eurjchem-1701	424	13	the	the	DET
eurjchem-1701	424	14	creative	creative	ADJ
eurjchem-1701	424	15	commons	common	NOUN
eurjchem-1701	424	16	attribution	attribution	NOUN
eurjchem-1701	424	17	-	-	PUNCT
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eurjchem-1701	424	19	commercial	commercial	NOUN
eurjchem-1701	424	20	(	(	PUNCT
eurjchem-1701	424	21	cc	cc	NOUN
eurjchem-1701	424	22	by	by	ADP
eurjchem-1701	424	23	nc	nc	PROPN
eurjchem-1701	424	24	)	)	PUNCT
eurjchem-1701	424	25	(	(	PUNCT
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eurjchem-1701	424	31	(	(	PUNCT
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eurjchem-1701	424	34	.	.	PUNCT
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eurjchem-1701	425	5	,	,	PUNCT
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eurjchem-1701	425	11	.	.	PUNCT
eurjchem-1701	426	1	this	this	PRON
eurjchem-1701	426	2	is	be	AUX
eurjchem-1701	426	3	an	an	DET
eurjchem-1701	426	4	open	open	ADJ
eurjchem-1701	426	5	access	access	NOUN
eurjchem-1701	426	6	article	article	NOUN
eurjchem-1701	426	7	distributed	distribute	VERB
eurjchem-1701	426	8	under	under	ADP
eurjchem-1701	426	9	the	the	DET
eurjchem-1701	426	10	terms	term	NOUN
eurjchem-1701	426	11	and	and	CCONJ
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eurjchem-1701	426	14	the	the	DET
eurjchem-1701	426	15	cc	cc	PROPN
eurjchem-1701	426	16	by	by	ADP
eurjchem-1701	426	17	nc	nc	PROPN
eurjchem-1701	426	18	license	license	PROPN
eurjchem-1701	426	19	,	,	PUNCT
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eurjchem-1701	426	21	permits	permit	VERB
eurjchem-1701	426	22	unrestricted	unrestricted	ADJ
eurjchem-1701	426	23	non	non	ADJ
eurjchem-1701	426	24	-	-	ADJ
eurjchem-1701	426	25	commercial	commercial	ADJ
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eurjchem-1701	426	27	,	,	PUNCT
eurjchem-1701	426	28	distribution	distribution	NOUN
eurjchem-1701	426	29	,	,	PUNCT
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eurjchem-1701	426	31	reproduction	reproduction	NOUN
eurjchem-1701	426	32	in	in	ADP
eurjchem-1701	426	33	any	any	DET
eurjchem-1701	426	34	medium	medium	NOUN
eurjchem-1701	426	35	,	,	PUNCT
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eurjchem-1701	426	37	the	the	DET
eurjchem-1701	426	38	original	original	ADJ
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eurjchem-1701	426	41	properly	properly	ADV
eurjchem-1701	426	42	cited	cite	VERB
eurjchem-1701	426	43	without	without	ADP
eurjchem-1701	426	44	any	any	DET
eurjchem-1701	426	45	further	further	ADJ
eurjchem-1701	426	46	permission	permission	NOUN
eurjchem-1701	426	47	from	from	ADP
eurjchem-1701	426	48	atlanta	atlanta	PROPN
eurjchem-1701	426	49	publishing	publishing	PROPN
eurjchem-1701	426	50	house	house	PROPN
eurjchem-1701	426	51	llc	llc	PROPN
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eurjchem-1701	426	57	)	)	PUNCT
eurjchem-1701	426	58	.	.	PUNCT
eurjchem-1701	427	1	no	no	DET
eurjchem-1701	427	2	use	use	NOUN
eurjchem-1701	427	3	,	,	PUNCT
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eurjchem-1701	427	12	comply	comply	VERB
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eurjchem-1701	427	16	.	.	PUNCT
eurjchem-1701	428	1	permissions	permission	NOUN
eurjchem-1701	428	2	for	for	ADP
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eurjchem-1701	428	4	use	use	NOUN
eurjchem-1701	428	5	of	of	ADP
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eurjchem-1701	428	7	work	work	NOUN
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eurjchem-1701	428	9	the	the	DET
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eurjchem-1701	428	11	of	of	ADP
eurjchem-1701	428	12	the	the	DET
eurjchem-1701	428	13	license	license	NOUN
eurjchem-1701	428	14	(	(	PUNCT
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eurjchem-1701	428	17	are	be	AUX
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eurjchem-1701	428	20	atlanta	atlanta	PROPN
eurjchem-1701	428	21	publishing	publishing	PROPN
eurjchem-1701	428	22	house	house	PROPN
eurjchem-1701	428	23	llc	llc	PROPN
eurjchem-1701	428	24	(	(	PUNCT
eurjchem-1701	428	25	european	european	PROPN
eurjchem-1701	428	26	journal	journal	PROPN
eurjchem-1701	428	27	of	of	ADP
eurjchem-1701	428	28	chemistry	chemistry	NOUN
eurjchem-1701	428	29	)	)	PUNCT
eurjchem-1701	428	30	.	.	PUNCT
eurjchem-1701	429	1	2018	2018	NUM
eurjchem-1701	429	2	–	–	PUNCT
eurjchem-1701	429	3	european	european	ADJ
eurjchem-1701	429	4	journal	journal	NOUN
eurjchem-1701	429	5	of	of	ADP
eurjchem-1701	429	6	chemistry	chemistry	NOUN
eurjchem-1701	429	7	–	–	PUNCT
eurjchem-1701	429	8	cc	cc	NOUN
eurjchem-1701	429	9	by	by	ADP
eurjchem-1701	429	10	nc	nc	PROPN
eurjchem-1701	429	11	–	–	PUNCT
eurjchem-1701	429	12	doi	doi	NOUN
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eurjchem-1701	429	17	-	-	PUNCT
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eurjchem-1701	429	22	http://www.eurjchem.com/index.php/eurjchem/pages/view/terms	http://www.eurjchem.com/index.php/eurjchem/pages/view/term	NOUN
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eurjchem-1701	429	24	.	.	PUNCT
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eurjchem-1701	432	7	-	-	PUNCT
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eurjchem-1701	432	9	hydrochloride	hydrochloride	NOUN
eurjchem-1701	432	10	(	(	PUNCT
eurjchem-1701	432	11	2	2	NUM
eurjchem-1701	432	12	)	)	PUNCT
eurjchem-1701	432	13	2.3.2	2.3.2	NUM
eurjchem-1701	432	14	.	.	PUNCT
eurjchem-1701	433	1	synthesis	synthesis	NOUN
eurjchem-1701	433	2	of	of	ADP
eurjchem-1701	433	3	2	2	NUM
eurjchem-1701	433	4	-	-	PUNCT
eurjchem-1701	433	5	hydrazinyl-6-(thiophen-2	hydrazinyl-6-(thiophen-2	NOUN
eurjchem-1701	433	6	-	-	PUNCT
eurjchem-1701	433	7	yl)-4h-1,3,5	yl)-4h-1,3,5	NOUN
eurjchem-1701	433	8	-	-	PUNCT
eurjchem-1701	433	9	oxadiazine-4	oxadiazine-4	PRON
eurjchem-1701	433	10	-	-	PUNCT
eurjchem-1701	433	11	thione	thione	ADJ
eurjchem-1701	433	12	(	(	PUNCT
eurjchem-1701	433	13	3	3	NUM
eurjchem-1701	433	14	)	)	PUNCT
eurjchem-1701	433	15	2.3.3	2.3.3	NUM
eurjchem-1701	433	16	.	.	PUNCT
eurjchem-1701	434	1	synthesis	synthesis	NOUN
eurjchem-1701	434	2	of	of	ADP
eurjchem-1701	434	3	1,2	1,2	NUM
eurjchem-1701	434	4	-	-	PUNCT
eurjchem-1701	434	5	dihydro-1	dihydro-1	NUM
eurjchem-1701	434	6	-	-	PUNCT
eurjchem-1701	434	7	phenyl-5-(thiophen-2	phenyl-5-(thiophen-2	NOUN
eurjchem-1701	434	8	-	-	PUNCT
eurjchem-1701	434	9	yl)-1	yl)-1	NOUN
eurjchem-1701	434	10	,	,	PUNCT
eurjchem-1701	434	11	2,4	2,4	NUM
eurjchem-1701	434	12	-	-	PUNCT
eurjchem-1701	434	13	triazole-3	triazole-3	NOUN
eurjchem-1701	434	14	-	-	PUNCT
eurjchem-1701	434	15	thione	thione	NOUN
eurjchem-1701	434	16	(	(	PUNCT
eurjchem-1701	434	17	4	4	NUM
eurjchem-1701	434	18	)	)	PUNCT
eurjchem-1701	434	19	2.3.4	2.3.4	NUM
eurjchem-1701	434	20	.	.	PUNCT
eurjchem-1701	435	1	synthesis	synthesis	NOUN
eurjchem-1701	435	2	of	of	ADP
eurjchem-1701	435	3	n-(1	n-(1	NOUN
eurjchem-1701	435	4	-	-	PUNCT
eurjchem-1701	435	5	phenylhydrazinecarbonothioyl)thiophene-2	phenylhydrazinecarbonothioyl)thiophene-2	PRON
eurjchem-1701	435	6	-	-	PUNCT
eurjchem-1701	435	7	carboxamide	carboxamide	NOUN
eurjchem-1701	435	8	hydrochloride	hydrochloride	NOUN
eurjchem-1701	435	9	(	(	PUNCT
eurjchem-1701	435	10	5	5	NUM
eurjchem-1701	435	11	)	)	PUNCT
eurjchem-1701	435	12	2.3.5	2.3.5	NUM
eurjchem-1701	435	13	.	.	PUNCT
eurjchem-1701	436	1	synthesis	synthesis	NOUN
eurjchem-1701	436	2	of	of	ADP
eurjchem-1701	436	3	n-(6	n-(6	NOUN
eurjchem-1701	436	4	-	-	PUNCT
eurjchem-1701	436	5	oxo-2	oxo-2	NOUN
eurjchem-1701	436	6	-	-	PUNCT
eurjchem-1701	436	7	phenyl-5,6	phenyl-5,6	NOUN
eurjchem-1701	436	8	-	-	PUNCT
eurjchem-1701	436	9	dihydro-1h	dihydro-1h	NOUN
eurjchem-1701	436	10	-	-	PUNCT
eurjchem-1701	436	11	furo[2,3	furo[2,3	ADJ
eurjchem-1701	436	12	-	-	PUNCT
eurjchem-1701	436	13	e][1,3,4]thiadiazin-3(2h)-ylidene)thiophene-2	e][1,3,4]thiadiazin-3(2h)-ylidene)thiophene-2	NOUN
eurjchem-1701	436	14	-	-	PUNCT
eurjchem-1701	436	15	carboxamide	carboxamide	NOUN
eurjchem-1701	436	16	(	(	PUNCT
eurjchem-1701	436	17	6	6	NUM
eurjchem-1701	436	18	)	)	PUNCT
eurjchem-1701	436	19	2.3.6	2.3.6	NUM
eurjchem-1701	436	20	.	.	PUNCT
eurjchem-1701	437	1	synthesis	synthesis	NOUN
eurjchem-1701	437	2	of	of	ADP
eurjchem-1701	437	3	n-(5	n-(5	PROPN
eurjchem-1701	437	4	-	-	PUNCT
eurjchem-1701	437	5	hydroxy-3	hydroxy-3	PROPN
eurjchem-1701	437	6	-	-	PUNCT
eurjchem-1701	437	7	phenyl-3,6	phenyl-3,6	ADP
eurjchem-1701	437	8	-	-	PUNCT
eurjchem-1701	437	9	dihydro-2h-1,3,4	dihydro-2h-1,3,4	ADJ
eurjchem-1701	437	10	-	-	PUNCT
eurjchem-1701	437	11	thiadiazin-2	thiadiazin-2	NUM
eurjchem-1701	437	12	-	-	PUNCT
eurjchem-1701	437	13	ylidene)thiophene-2	ylidene)thiophene-2	NOUN
eurjchem-1701	437	14	-	-	PUNCT
eurjchem-1701	437	15	carboxamide	carboxamide	NOUN
eurjchem-1701	437	16	(	(	PUNCT
eurjchem-1701	437	17	7	7	NUM
eurjchem-1701	437	18	)	)	PUNCT
eurjchem-1701	437	19	2.3.7	2.3.7	NUM
eurjchem-1701	437	20	.	.	PUNCT
eurjchem-1701	438	1	synthesis	synthesis	NOUN
eurjchem-1701	438	2	of	of	ADP
eurjchem-1701	438	3	1,2	1,2	NUM
eurjchem-1701	438	4	-	-	PUNCT
eurjchem-1701	438	5	dihydro-2	dihydro-2	NUM
eurjchem-1701	438	6	-	-	PUNCT
eurjchem-1701	438	7	phenyl-5-(thiophen-2	phenyl-5-(thiophen-2	NOUN
eurjchem-1701	438	8	-	-	PUNCT
eurjchem-1701	438	9	yl)-1,2,4	yl)-1,2,4	ADV
eurjchem-1701	438	10	-	-	PUNCT
eurjchem-1701	438	11	triazole-3	triazole-3	NOUN
eurjchem-1701	438	12	-	-	PUNCT
eurjchem-1701	438	13	thione	thione	NOUN
eurjchem-1701	438	14	(	(	PUNCT
eurjchem-1701	438	15	8)	8)	NOUN
eurjchem-1701	438	16	2.3.8	2.3.8	NUM
eurjchem-1701	438	17	.	.	PUNCT
eurjchem-1701	439	1	synthesis	synthesis	NOUN
eurjchem-1701	439	2	of	of	ADP
eurjchem-1701	439	3	n-(2	n-(2	PROPN
eurjchem-1701	439	4	-	-	PUNCT
eurjchem-1701	439	5	isonicotinoylhydrazinecarbonothio	isonicotinoylhydrazinecarbonothio	NOUN
eurjchem-1701	439	6	-	-	PUNCT
eurjchem-1701	439	7	yl)thiophene-2	yl)thiophene-2	NOUN
eurjchem-1701	439	8	-	-	PUNCT
eurjchem-1701	439	9	carboxamide	carboxamide	NOUN
eurjchem-1701	439	10	(	(	PUNCT
eurjchem-1701	439	11	11	11	NUM
eurjchem-1701	439	12	)	)	PUNCT
eurjchem-1701	439	13	2.3.9	2.3.9	NUM
eurjchem-1701	439	14	.	.	PUNCT
eurjchem-1701	440	1	synthesis	synthesis	NOUN
eurjchem-1701	440	2	of	of	ADP
eurjchem-1701	440	3	n-(5-(pyridin-4	n-(5-(pyridin-4	NOUN
eurjchem-1701	440	4	-	-	PUNCT
eurjchem-1701	440	5	yl)-1,3,4	yl)-1,3,4	NOUN
eurjchem-1701	440	6	-	-	PUNCT
eurjchem-1701	440	7	thiadiazol-2	thiadiazol-2	NUM
eurjchem-1701	440	8	-	-	PUNCT
eurjchem-1701	440	9	yl)thiophene-2	yl)thiophene-2	NOUN
eurjchem-1701	440	10	-	-	PUNCT
eurjchem-1701	440	11	carboxamide	carboxamide	NOUN
eurjchem-1701	440	12	(	(	PUNCT
eurjchem-1701	440	13	12	12	NUM
eurjchem-1701	440	14	)	)	PUNCT
eurjchem-1701	440	15	2.3.10	2.3.10	NOUN
eurjchem-1701	440	16	.	.	PUNCT
eurjchem-1701	441	1	synthesis	synthesis	NOUN
eurjchem-1701	441	2	of	of	ADP
eurjchem-1701	441	3	(	(	PUNCT
eurjchem-1701	441	4	3	3	NUM
eurjchem-1701	441	5	-	-	PUNCT
eurjchem-1701	441	6	mercapto-5-(pyridin-4	mercapto-5-(pyridin-4	NOUN
eurjchem-1701	441	7	-	-	PUNCT
eurjchem-1701	441	8	yl)-4h-1,2,4	yl)-4h-1,2,4	NOUN
eurjchem-1701	441	9	-	-	PUNCT
eurjchem-1701	441	10	triazol-4	triazol-4	NUM
eurjchem-1701	441	11	-	-	PUNCT
eurjchem-1701	441	12	yl)(thiophen-2	yl)(thiophen-2	NOUN
eurjchem-1701	441	13	-	-	ADJ
eurjchem-1701	441	14	yl)methanone	yl)methanone	NOUN
eurjchem-1701	441	15	(	(	PUNCT
eurjchem-1701	441	16	13	13	NUM
eurjchem-1701	441	17	)	)	PUNCT
eurjchem-1701	441	18	2.3.11	2.3.11	NOUN
eurjchem-1701	441	19	.	.	PUNCT
eurjchem-1701	442	1	synthesis	synthesis	NOUN
eurjchem-1701	442	2	of	of	ADP
eurjchem-1701	442	3	5-(pyridin-4	5-(pyridin-4	NUM
eurjchem-1701	442	4	-	-	ADJ
eurjchem-1701	442	5	yl)-2h-1,2,4	yl)-2h-1,2,4	NOUN
eurjchem-1701	442	6	-	-	PUNCT
eurjchem-1701	442	7	triazole-3(4h)-thione	triazole-3(4h)-thione	NOUN
eurjchem-1701	442	8	(	(	PUNCT
eurjchem-1701	442	9	14	14	NUM
eurjchem-1701	442	10	)	)	PUNCT
eurjchem-1701	442	11	2.3.12	2.3.12	NUM
eurjchem-1701	442	12	.	.	PUNCT
eurjchem-1701	442	13	synthesis	synthesis	NOUN
eurjchem-1701	442	14	of	of	ADP
eurjchem-1701	442	15	ethyl	ethyl	PROPN
eurjchem-1701	442	16	2-(3-(thiophene-2	2-(3-(thiophene-2	NUM
eurjchem-1701	442	17	-	-	PUNCT
eurjchem-1701	442	18	carbonyl)thiou	carbonyl)thiou	VERB
eurjchem-1701	442	19	-	-	PUNCT
eurjchem-1701	442	20	reido)-4,5,6,7	reido)-4,5,6,7	NOUN
eurjchem-1701	442	21	-	-	PUNCT
eurjchem-1701	442	22	tetrahydrobenzo[b]thiophene-3	tetrahydrobenzo[b]thiophene-3	NOUN
eurjchem-1701	442	23	-	-	PUNCT
eurjchem-1701	442	24	carboxylate	carboxylate	NOUN
eurjchem-1701	442	25	(	(	PUNCT
eurjchem-1701	442	26	15	15	NUM
eurjchem-1701	442	27	)	)	PUNCT
eurjchem-1701	442	28	2.3.13	2.3.13	NUM
eurjchem-1701	442	29	.	.	PUNCT
eurjchem-1701	443	1	synthesis	synthesis	NOUN
eurjchem-1701	443	2	of	of	ADP
eurjchem-1701	443	3	2-(3-(thiophene-2	2-(3-(thiophene-2	NUM
eurjchem-1701	443	4	-	-	PUNCT
eurjchem-1701	443	5	carbonyl)thioureido)-4,5,6,7	carbonyl)thioureido)-4,5,6,7	NOUN
eurjchem-1701	443	6	-	-	PUNCT
eurjchem-1701	443	7	tetrahydrobenzo[b]thiophene-3	tetrahydrobenzo[b]thiophene-3	NOUN
eurjchem-1701	443	8	-	-	PUNCT
eurjchem-1701	443	9	carboxylic	carboxylic	ADJ
eurjchem-1701	443	10	acid	acid	NOUN
eurjchem-1701	443	11	(	(	PUNCT
eurjchem-1701	443	12	16	16	NUM
eurjchem-1701	443	13	)	)	PUNCT
eurjchem-1701	443	14	2.3.14	2.3.14	NUM
eurjchem-1701	443	15	.	.	PUNCT
eurjchem-1701	444	1	synthesis	synthesis	NOUN
eurjchem-1701	444	2	of	of	ADP
eurjchem-1701	444	3	10	10	NUM
eurjchem-1701	444	4	-	-	PUNCT
eurjchem-1701	444	5	amino-2-(thiophen-2	amino-2-(thiophen-2	NOUN
eurjchem-1701	444	6	-	-	PUNCT
eurjchem-1701	444	7	yl)-4	yl)-4	VERB
eurjchem-1701	444	8	-	-	PUNCT
eurjchem-1701	444	9	thioxo-4h	thioxo-4h	NUM
eurjchem-1701	444	10	-	-	PUNCT
eurjchem-1701	444	11	naphtho[2,3	naphtho[2,3	NUM
eurjchem-1701	444	12	-	-	PUNCT
eurjchem-1701	444	13	e][1,3]oxazine-5	e][1,3]oxazine-5	ADJ
eurjchem-1701	444	14	-	-	PUNCT
eurjchem-1701	444	15	sulfonic	sulfonic	ADJ
eurjchem-1701	444	16	acid	acid	NOUN
eurjchem-1701	444	17	(	(	PUNCT
eurjchem-1701	444	18	18	18	NUM
eurjchem-1701	444	19	)	)	PUNCT
eurjchem-1701	444	20	2.3.15	2.3.15	NUM
eurjchem-1701	444	21	.	.	PUNCT
eurjchem-1701	444	22	synthesis	synthesis	NOUN
eurjchem-1701	444	23	of	of	ADP
eurjchem-1701	444	24	n-(4,5	n-(4,5	NOUN
eurjchem-1701	444	25	-	-	PUNCT
eurjchem-1701	444	26	dihydro-1-(sulfanylene(thiophe	dihydro-1-(sulfanylene(thiophe	NOUN
eurjchem-1701	444	27	-	-	PUNCT
eurjchem-1701	444	28	ne-2	ne-2	CCONJ
eurjchem-1701	444	29	-	-	PUNCT
eurjchem-1701	444	30	carboxamido)methyl)-1h	carboxamido)methyl)-1h	NOUN
eurjchem-1701	444	31	-	-	PUNCT
eurjchem-1701	444	32	imidazol-2	imidazol-2	NUM
eurjchem-1701	444	33	-	-	PUNCT
eurjchem-1701	444	34	yl)thiophene-2	yl)thiophene-2	NOUN
eurjchem-1701	444	35	-	-	PUNCT
eurjchem-1701	444	36	carboxamide	carboxamide	NOUN
eurjchem-1701	444	37	(	(	PUNCT
eurjchem-1701	444	38	19	19	NUM
eurjchem-1701	444	39	)	)	PUNCT
eurjchem-1701	444	40	2.4	2.4	NUM
eurjchem-1701	444	41	.	.	PUNCT
eurjchem-1701	445	1	antitumor	antitumor	PROPN
eurjchem-1701	445	2	activity	activity	NOUN
eurjchem-1701	445	3	test	test	NOUN
eurjchem-1701	445	4	tumor	tumor	NOUN
eurjchem-1701	445	5	cell	cell	NOUN
eurjchem-1701	445	6	growth	growth	NOUN
eurjchem-1701	445	7	assay	assay	VERB
eurjchem-1701	445	8	3	3	NUM
eurjchem-1701	445	9	.	.	NOUN
eurjchem-1701	445	10	results	result	NOUN
eurjchem-1701	445	11	and	and	CCONJ
eurjchem-1701	445	12	discussion	discussion	NOUN
eurjchem-1701	445	13	3.1	3.1	NUM
eurjchem-1701	445	14	.	.	PUNCT
eurjchem-1701	446	1	chemistry	chemistry	NOUN
eurjchem-1701	446	2	3.2	3.2	NUM
eurjchem-1701	446	3	.	.	PUNCT
eurjchem-1701	447	1	antitumor	antitumor	NOUN
eurjchem-1701	447	2	activity	activity	NOUN
eurjchem-1701	447	3	4	4	NUM
eurjchem-1701	447	4	.	.	PUNCT
eurjchem-1701	448	1	conclusion	conclusion	NOUN
eurjchem-1701	448	2	disclosure	disclosure	NOUN
eurjchem-1701	448	3	statement	statement	NOUN
eurjchem-1701	448	4	orcid	orcid	PROPN
eurjchem-1701	448	5	references	reference	NOUN
eurjchem-1701	448	6	printfield10	printfield10	NOUN
eurjchem-1701	448	7	:	:	PUNCT
eurjchem-1701	448	8	printfield11	printfield11	NOUN
eurjchem-1701	448	9	:	:	PUNCT
eurjchem-1701	448	10	printfield12	printfield12	PROPN
eurjchem-1701	448	11	:	:	PUNCT
eurjchem-1701	448	12	printfield13	printfield13	VERB
eurjchem-1701	448	13	:	:	PUNCT
eurjchem-1701	448	14	printfield14	printfield14	NOUN
eurjchem-1701	448	15	:	:	PUNCT
eurjchem-1701	448	16	printfield15	printfield15	NOUN
eurjchem-1701	448	17	:	:	PUNCT
eurjchem-1701	448	18	printfield16	printfield16	ADJ
eurjchem-1701	448	19	:	:	PUNCT
eurjchem-1701	448	20	printfield17	printfield17	NOUN
eurjchem-1701	448	21	:	:	PUNCT
eurjchem-1701	448	22	printfield20	printfield20	PROPN
eurjchem-1701	448	23	:	:	PUNCT
eurjchem-1701	448	24	printfield21	printfield21	ADJ
eurjchem-1701	448	25	:	:	PUNCT
eurjchem-1701	448	26	printfield22	printfield22	NOUN
eurjchem-1701	448	27	:	:	PUNCT
eurjchem-1701	448	28	printfield23	printfield23	NOUN
eurjchem-1701	448	29	:	:	PUNCT
eurjchem-1701	448	30	printfield24	printfield24	NOUN
eurjchem-1701	448	31	:	:	PUNCT
eurjchem-1701	448	32	printfield25	printfield25	NOUN
eurjchem-1701	448	33	:	:	PUNCT
eurjchem-1701	448	34	printfield26	printfield26	ADJ
eurjchem-1701	448	35	:	:	PUNCT
eurjchem-1701	448	36	printfield27	printfield27	NOUN
eurjchem-1701	448	37	:	:	PUNCT