id	sid	tid	token	lemma	pos
eurjchem-1783	1	1	a	a	DET
eurjchem-1783	1	2	novel	novel	ADJ
eurjchem-1783	1	3	and	and	CCONJ
eurjchem-1783	1	4	expeditious	expeditious	ADJ
eurjchem-1783	1	5	synthesis	synthesis	NOUN
eurjchem-1783	1	6	of	of	ADP
eurjchem-1783	1	7	oxazolidinone	oxazolidinone	NOUN
eurjchem-1783	1	8	drugs	drug	NOUN
eurjchem-1783	1	9	linezolid	linezolid	NOUN
eurjchem-1783	1	10	and	and	CCONJ
eurjchem-1783	1	11	eperezolid	eperezolid	PROPN
eurjchem-1783	1	12	european	european	PROPN
eurjchem-1783	1	13	journal	journal	PROPN
eurjchem-1783	1	14	of	of	ADP
eurjchem-1783	1	15	chemistry	chemistry	NOUN
eurjchem-1783	1	16	9	9	NUM
eurjchem-1783	1	17	(	(	PUNCT
eurjchem-1783	1	18	4	4	NUM
eurjchem-1783	1	19	)	)	PUNCT
eurjchem-1783	1	20	(	(	PUNCT
eurjchem-1783	1	21	2018	2018	NUM
eurjchem-1783	1	22	)	)	PUNCT
eurjchem-1783	1	23	353	353	NUM
eurjchem-1783	1	24	-	-	SYM
eurjchem-1783	1	25	359	359	NUM
eurjchem-1783	1	26	european	european	ADJ
eurjchem-1783	1	27	journal	journal	PROPN
eurjchem-1783	1	28	of	of	ADP
eurjchem-1783	1	29	chemistry	chemistry	NOUN
eurjchem-1783	1	30	view	view	NOUN
eurjchem-1783	1	31	journal	journal	PROPN
eurjchem-1783	1	32	online	online	PROPN
eurjchem-1783	1	33	view	view	NOUN
eurjchem-1783	1	34	article	article	NOUN
eurjchem-1783	1	35	online	online	VERB
eurjchem-1783	1	36	a	a	DET
eurjchem-1783	1	37	novel	novel	ADJ
eurjchem-1783	1	38	and	and	CCONJ
eurjchem-1783	1	39	expeditious	expeditious	ADJ
eurjchem-1783	1	40	synthesis	synthesis	NOUN
eurjchem-1783	1	41	of	of	ADP
eurjchem-1783	1	42	oxazolidinone	oxazolidinone	NOUN
eurjchem-1783	1	43	drugs	drug	NOUN
eurjchem-1783	1	44	linezolid	linezolid	NOUN
eurjchem-1783	1	45	and	and	CCONJ
eurjchem-1783	1	46	eperezolid	eperezolid	NOUN
eurjchem-1783	1	47	ranjith	ranjith	PROPN
eurjchem-1783	1	48	siddaraj	siddaraj	ADJ
eurjchem-1783	1	49	1	1	NUM
eurjchem-1783	1	50	,	,	PUNCT
eurjchem-1783	1	51	shivaraja	shivaraja	NOUN
eurjchem-1783	1	52	govindaiah	govindaiah	PROPN
eurjchem-1783	1	53	2	2	NUM
eurjchem-1783	1	54	,	,	PUNCT
eurjchem-1783	1	55	raghu	raghu	PROPN
eurjchem-1783	1	56	ningegowda	ningegowda	PROPN
eurjchem-1783	1	57	1	1	NUM
eurjchem-1783	1	58	,	,	PUNCT
eurjchem-1783	1	59	nanjunda	nanjunda	ADJ
eurjchem-1783	1	60	swamy	swamy	PROPN
eurjchem-1783	1	61	shivananju	shivananju	PROPN
eurjchem-1783	1	62	3	3	NUM
eurjchem-1783	1	63	and	and	CCONJ
eurjchem-1783	1	64	babu	babu	PROPN
eurjchem-1783	1	65	shubha	shubha	PROPN
eurjchem-1783	1	66	priya	priya	PROPN
eurjchem-1783	1	67	1	1	NUM
eurjchem-1783	1	68	,	,	PUNCT
eurjchem-1783	1	69	*	*	PROPN
eurjchem-1783	1	70	1	1	NUM
eurjchem-1783	1	71	department	department	NOUN
eurjchem-1783	1	72	of	of	ADP
eurjchem-1783	1	73	studies	study	NOUN
eurjchem-1783	1	74	in	in	ADP
eurjchem-1783	1	75	chemistry	chemistry	NOUN
eurjchem-1783	1	76	,	,	PUNCT
eurjchem-1783	1	77	university	university	NOUN
eurjchem-1783	1	78	of	of	ADP
eurjchem-1783	1	79	mysore	mysore	PROPN
eurjchem-1783	1	80	,	,	PUNCT
eurjchem-1783	1	81	manasagangotri	manasagangotri	NOUN
eurjchem-1783	1	82	,	,	PUNCT
eurjchem-1783	1	83	mysore-570006	mysore-570006	ADJ
eurjchem-1783	1	84	,	,	PUNCT
eurjchem-1783	1	85	karnataka	karnataka	PROPN
eurjchem-1783	1	86	,	,	PUNCT
eurjchem-1783	1	87	india	india	PROPN
eurjchem-1783	1	88	ranjithsiddaraj@yahoo.co.in	ranjithsiddaraj@yahoo.co.in	PROPN
eurjchem-1783	1	89	(	(	PUNCT
eurjchem-1783	1	90	r.s	r.s	PROPN
eurjchem-1783	1	91	.	.	PROPN
eurjchem-1783	1	92	)	)	PUNCT
eurjchem-1783	1	93	,	,	PUNCT
eurjchem-1783	1	94	raghu.ningegowda80@gmail.com	raghu.ningegowda80@gmail.com	X
eurjchem-1783	1	95	(	(	PUNCT
eurjchem-1783	1	96	r.n	r.n	PROPN
eurjchem-1783	1	97	.	.	PROPN
eurjchem-1783	1	98	)	)	PUNCT
eurjchem-1783	1	99	,	,	PUNCT
eurjchem-1783	1	100	priyabs_chem@yahoo.com	priyabs_chem@yahoo.com	X
eurjchem-1783	1	101	(	(	PUNCT
eurjchem-1783	1	102	b.s.p	b.s.p	PROPN
eurjchem-1783	1	103	.	.	PUNCT
eurjchem-1783	1	104	)	)	PUNCT
eurjchem-1783	2	1	2	2	NUM
eurjchem-1783	2	2	department	department	NOUN
eurjchem-1783	2	3	of	of	ADP
eurjchem-1783	2	4	studies	study	NOUN
eurjchem-1783	2	5	and	and	CCONJ
eurjchem-1783	2	6	research	research	NOUN
eurjchem-1783	2	7	in	in	ADP
eurjchem-1783	2	8	chemistry	chemistry	NOUN
eurjchem-1783	2	9	,	,	PUNCT
eurjchem-1783	2	10	tumkur	tumkur	PROPN
eurjchem-1783	2	11	university	university	PROPN
eurjchem-1783	2	12	,	,	PUNCT
eurjchem-1783	2	13	tumkur-572103	tumkur-572103	NOUN
eurjchem-1783	2	14	,	,	PUNCT
eurjchem-1783	2	15	karnataka	karnataka	PROPN
eurjchem-1783	2	16	,	,	PUNCT
eurjchem-1783	2	17	india	india	PROPN
eurjchem-1783	2	18	shivarajchemtumkur@gmail.com	shivarajchemtumkur@gmail.com	PROPN
eurjchem-1783	2	19	(	(	PUNCT
eurjchem-1783	2	20	s.g	s.g	PROPN
eurjchem-1783	2	21	.	.	PROPN
eurjchem-1783	2	22	)	)	PUNCT
eurjchem-1783	2	23	3	3	NUM
eurjchem-1783	2	24	department	department	NOUN
eurjchem-1783	2	25	of	of	ADP
eurjchem-1783	2	26	biotechnology	biotechnology	NOUN
eurjchem-1783	2	27	,	,	PUNCT
eurjchem-1783	2	28	sri	sri	PROPN
eurjchem-1783	2	29	jayachamarajendra	jayachamarajendra	PROPN
eurjchem-1783	2	30	college	college	PROPN
eurjchem-1783	2	31	of	of	ADP
eurjchem-1783	2	32	engineering	engineering	PROPN
eurjchem-1783	2	33	,	,	PUNCT
eurjchem-1783	2	34	jss	jss	PROPN
eurjchem-1783	2	35	technical	technical	PROPN
eurjchem-1783	2	36	institutions	institutions	PROPN
eurjchem-1783	2	37	campus	campus	NOUN
eurjchem-1783	2	38	,	,	PUNCT
eurjchem-1783	2	39	mysore-570006	mysore-570006	ADJ
eurjchem-1783	2	40	,	,	PUNCT
eurjchem-1783	2	41	karnataka	karnataka	PROPN
eurjchem-1783	2	42	,	,	PUNCT
eurjchem-1783	2	43	india	india	PROPN
eurjchem-1783	2	44	nanju_chem@yahoo.com	nanju_chem@yahoo.com	PROPN
eurjchem-1783	2	45	(	(	PUNCT
eurjchem-1783	2	46	n.s.s	n.s.	NOUN
eurjchem-1783	2	47	.	.	PUNCT
eurjchem-1783	2	48	)	)	PUNCT
eurjchem-1783	3	1	*	*	PUNCT
eurjchem-1783	3	2	corresponding	correspond	VERB
eurjchem-1783	3	3	author	author	NOUN
eurjchem-1783	3	4	at	at	ADP
eurjchem-1783	3	5	:	:	PUNCT
eurjchem-1783	3	6	department	department	NOUN
eurjchem-1783	3	7	of	of	ADP
eurjchem-1783	3	8	studies	study	NOUN
eurjchem-1783	3	9	in	in	ADP
eurjchem-1783	3	10	chemistry	chemistry	NOUN
eurjchem-1783	3	11	,	,	PUNCT
eurjchem-1783	3	12	university	university	NOUN
eurjchem-1783	3	13	of	of	ADP
eurjchem-1783	3	14	mysore	mysore	PROPN
eurjchem-1783	3	15	,	,	PUNCT
eurjchem-1783	3	16	manasagangotri	manasagangotri	NOUN
eurjchem-1783	3	17	,	,	PUNCT
eurjchem-1783	3	18	mysore-570006	mysore-570006	ADJ
eurjchem-1783	3	19	,	,	PUNCT
eurjchem-1783	3	20	karnataka	karnataka	PROPN
eurjchem-1783	3	21	,	,	PUNCT
eurjchem-1783	3	22	india	india	PROPN
eurjchem-1783	3	23	.	.	PUNCT
eurjchem-1783	4	1	tel	tel	ADP
eurjchem-1783	4	2	:	:	PUNCT
eurjchem-1783	4	3	+91.821.2419448	+91.821.2419448	PUNCT
eurjchem-1783	4	4	fax	fax	NOUN
eurjchem-1783	4	5	:	:	PUNCT
eurjchem-1783	4	6	+91.821.2419363	+91.821.2419363	PUNCT
eurjchem-1783	4	7	e	e	X
eurjchem-1783	4	8	-	-	NOUN
eurjchem-1783	4	9	mail	mail	NOUN
eurjchem-1783	4	10	:	:	PUNCT
eurjchem-1783	4	11	priyabs_chem@yahoo.com	priyabs_chem@yahoo.com	X
eurjchem-1783	4	12	(	(	PUNCT
eurjchem-1783	4	13	b.s	b.s	PROPN
eurjchem-1783	4	14	.	.	PROPN
eurjchem-1783	4	15	priya	priya	PROPN
eurjchem-1783	4	16	)	)	PUNCT
eurjchem-1783	4	17	.	.	PUNCT
eurjchem-1783	5	1	10.5155	10.5155	NUM
eurjchem-1783	5	2	/	/	SYM
eurjchem-1783	5	3	eurjchem.9.4.353	eurjchem.9.4.353	PROPN
eurjchem-1783	5	4	-	-	PUNCT
eurjchem-1783	5	5	359.1783	359.1783	NUM
eurjchem-1783	5	6	received	receive	VERB
eurjchem-1783	5	7	:	:	PUNCT
eurjchem-1783	5	8	28	28	NUM
eurjchem-1783	5	9	august	august	PROPN
eurjchem-1783	5	10	2018	2018	NUM
eurjchem-1783	5	11	received	receive	VERB
eurjchem-1783	5	12	in	in	ADP
eurjchem-1783	5	13	revised	revise	VERB
eurjchem-1783	5	14	form	form	NOUN
eurjchem-1783	5	15	:	:	PUNCT
eurjchem-1783	5	16	04	04	NUM
eurjchem-1783	5	17	october	october	NOUN
eurjchem-1783	5	18	2018	2018	NUM
eurjchem-1783	5	19	accepted	accept	VERB
eurjchem-1783	5	20	:	:	PUNCT
eurjchem-1783	5	21	06	06	NUM
eurjchem-1783	5	22	october	october	PROPN
eurjchem-1783	5	23	2018	2018	NUM
eurjchem-1783	5	24	published	publish	VERB
eurjchem-1783	5	25	online	online	ADV
eurjchem-1783	5	26	:	:	PUNCT
eurjchem-1783	5	27	31	31	NUM
eurjchem-1783	5	28	december	december	PROPN
eurjchem-1783	5	29	2018	2018	NUM
eurjchem-1783	5	30	printed	print	VERB
eurjchem-1783	5	31	:	:	PUNCT
eurjchem-1783	5	32	31	31	NUM
eurjchem-1783	5	33	december	december	PROPN
eurjchem-1783	5	34	2018	2018	NUM
eurjchem-1783	5	35	a	a	DET
eurjchem-1783	5	36	concise	concise	ADJ
eurjchem-1783	5	37	and	and	CCONJ
eurjchem-1783	5	38	efficient	efficient	ADJ
eurjchem-1783	5	39	synthesis	synthesis	NOUN
eurjchem-1783	5	40	of	of	ADP
eurjchem-1783	5	41	linezolid	linezolid	NOUN
eurjchem-1783	5	42	and	and	CCONJ
eurjchem-1783	5	43	eperezolid	eperezolid	NOUN
eurjchem-1783	5	44	were	be	AUX
eurjchem-1783	5	45	accomplished	accomplish	VERB
eurjchem-1783	5	46	through	through	ADP
eurjchem-1783	5	47	a	a	DET
eurjchem-1783	5	48	convergent	convergent	NOUN
eurjchem-1783	5	49	scheme	scheme	NOUN
eurjchem-1783	5	50	utilizing	utilize	VERB
eurjchem-1783	5	51	diverse	diverse	ADJ
eurjchem-1783	5	52	reaction	reaction	NOUN
eurjchem-1783	5	53	conditions	condition	NOUN
eurjchem-1783	5	54	.	.	PUNCT
eurjchem-1783	6	1	the	the	DET
eurjchem-1783	6	2	synthesis	synthesis	NOUN
eurjchem-1783	6	3	demonstrates	demonstrate	VERB
eurjchem-1783	6	4	utility	utility	NOUN
eurjchem-1783	6	5	of	of	ADP
eurjchem-1783	6	6	a	a	DET
eurjchem-1783	6	7	new	new	ADJ
eurjchem-1783	6	8	approach	approach	NOUN
eurjchem-1783	6	9	to	to	PART
eurjchem-1783	6	10	facilitate	facilitate	VERB
eurjchem-1783	6	11	the	the	DET
eurjchem-1783	6	12	expeditious	expeditious	ADJ
eurjchem-1783	6	13	construction	construction	NOUN
eurjchem-1783	6	14	of	of	ADP
eurjchem-1783	6	15	3	3	NUM
eurjchem-1783	6	16	-	-	PUNCT
eurjchem-1783	6	17	aryl-5-(substituted	aryl-5-(substitute	VERB
eurjchem-1783	6	18	methyl)2	methyl)2	NOUN
eurjchem-1783	6	19	-	-	PUNCT
eurjchem-1783	6	20	oxazolidinones	oxazolidinone	NOUN
eurjchem-1783	6	21	and	and	CCONJ
eurjchem-1783	6	22	easier	easy	ADJ
eurjchem-1783	6	23	insertion	insertion	NOUN
eurjchem-1783	6	24	of	of	ADP
eurjchem-1783	6	25	n	n	CCONJ
eurjchem-1783	6	26	-	-	PUNCT
eurjchem-1783	6	27	acetyl	acetyl	NOUN
eurjchem-1783	6	28	group	group	NOUN
eurjchem-1783	6	29	.	.	PUNCT
eurjchem-1783	7	1	this	this	DET
eurjchem-1783	7	2	new	new	ADJ
eurjchem-1783	7	3	approach	approach	NOUN
eurjchem-1783	7	4	offers	offer	VERB
eurjchem-1783	7	5	the	the	DET
eurjchem-1783	7	6	possibility	possibility	NOUN
eurjchem-1783	7	7	of	of	ADP
eurjchem-1783	7	8	accessing	access	VERB
eurjchem-1783	7	9	related	related	ADJ
eurjchem-1783	7	10	2	2	NUM
eurjchem-1783	7	11	-	-	PUNCT
eurjchem-1783	7	12	oxazolidinone	oxazolidinone	NUM
eurjchem-1783	7	13	members	member	NOUN
eurjchem-1783	7	14	easily	easily	ADV
eurjchem-1783	7	15	as	as	ADV
eurjchem-1783	7	16	well	well	ADV
eurjchem-1783	7	17	as	as	ADP
eurjchem-1783	7	18	making	make	VERB
eurjchem-1783	7	19	additional	additional	ADJ
eurjchem-1783	7	20	analogues	analogue	NOUN
eurjchem-1783	7	21	of	of	ADP
eurjchem-1783	7	22	linezolid	linezolid	NOUN
eurjchem-1783	7	23	.	.	PUNCT
eurjchem-1783	8	1	the	the	DET
eurjchem-1783	8	2	adopted	adopt	VERB
eurjchem-1783	8	3	method	method	NOUN
eurjchem-1783	8	4	afforded	afford	VERB
eurjchem-1783	8	5	high	high	ADJ
eurjchem-1783	8	6	purity	purity	NOUN
eurjchem-1783	8	7	and	and	CCONJ
eurjchem-1783	8	8	excellent	excellent	ADJ
eurjchem-1783	8	9	yield	yield	NOUN
eurjchem-1783	8	10	compared	compare	VERB
eurjchem-1783	8	11	to	to	ADP
eurjchem-1783	8	12	other	other	ADJ
eurjchem-1783	8	13	existing	exist	VERB
eurjchem-1783	8	14	synthetic	synthetic	ADJ
eurjchem-1783	8	15	methods	method	NOUN
eurjchem-1783	8	16	.	.	PUNCT
eurjchem-1783	9	1	the	the	DET
eurjchem-1783	9	2	compounds	compound	NOUN
eurjchem-1783	9	3	were	be	AUX
eurjchem-1783	9	4	successfully	successfully	ADV
eurjchem-1783	9	5	characterized	characterize	VERB
eurjchem-1783	9	6	by	by	ADP
eurjchem-1783	9	7	known	know	VERB
eurjchem-1783	9	8	spectroscopic	spectroscopic	NOUN
eurjchem-1783	9	9	techniques	technique	NOUN
eurjchem-1783	9	10	.	.	PUNCT
eurjchem-1783	10	1	linezolid	linezolid	PROPN
eurjchem-1783	10	2	eperezolid	eperezolid	PROPN
eurjchem-1783	10	3	acetamide	acetamide	NOUN
eurjchem-1783	10	4	sodium	sodium	PROPN
eurjchem-1783	10	5	iodide	iodide	NOUN
eurjchem-1783	10	6	cesium	cesium	NOUN
eurjchem-1783	10	7	carbonate	carbonate	NOUN
eurjchem-1783	10	8	(	(	PUNCT
eurjchem-1783	10	9	r)-2-(bromomethyl)oxirane	r)-2-(bromomethyl)oxirane	NOUN
eurjchem-1783	10	10	cite	cite	VERB
eurjchem-1783	10	11	this	this	PRON
eurjchem-1783	10	12	:	:	PUNCT
eurjchem-1783	10	13	eur	eur	PROPN
eurjchem-1783	10	14	.	.	PUNCT
eurjchem-1783	11	1	j.	j.	PROPN
eurjchem-1783	11	2	chem	chem	PROPN
eurjchem-1783	11	3	.	.	PUNCT
eurjchem-1783	12	1	2018	2018	NUM
eurjchem-1783	12	2	,	,	PUNCT
eurjchem-1783	12	3	9(4	9(4	NUM
eurjchem-1783	12	4	)	)	PUNCT
eurjchem-1783	12	5	,	,	PUNCT
eurjchem-1783	12	6	353	353	NUM
eurjchem-1783	12	7	-	-	SYM
eurjchem-1783	12	8	359	359	NUM
eurjchem-1783	12	9	journal	journal	NOUN
eurjchem-1783	12	10	website	website	NOUN
eurjchem-1783	12	11	:	:	PUNCT
eurjchem-1783	12	12	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1783	12	13	1	1	X
eurjchem-1783	12	14	.	.	PUNCT
eurjchem-1783	12	15	introduction	introduction	NOUN
eurjchem-1783	12	16	oxazolidinones	oxazolidinone	NOUN
eurjchem-1783	12	17	represent	represent	VERB
eurjchem-1783	12	18	a	a	DET
eurjchem-1783	12	19	class	class	NOUN
eurjchem-1783	12	20	of	of	ADP
eurjchem-1783	12	21	versatile	versatile	ADJ
eurjchem-1783	12	22	compounds	compound	NOUN
eurjchem-1783	12	23	in	in	ADP
eurjchem-1783	12	24	antibacterial	antibacterial	ADJ
eurjchem-1783	12	25	research	research	NOUN
eurjchem-1783	12	26	because	because	SCONJ
eurjchem-1783	12	27	they	they	PRON
eurjchem-1783	12	28	represent	represent	VERB
eurjchem-1783	12	29	the	the	DET
eurjchem-1783	12	30	first	first	ADJ
eurjchem-1783	12	31	members	member	NOUN
eurjchem-1783	12	32	of	of	ADP
eurjchem-1783	12	33	antibiotics	antibiotic	NOUN
eurjchem-1783	12	34	to	to	PART
eurjchem-1783	12	35	enter	enter	VERB
eurjchem-1783	12	36	clinical	clinical	ADJ
eurjchem-1783	12	37	availability	availability	NOUN
eurjchem-1783	12	38	over	over	ADP
eurjchem-1783	12	39	the	the	DET
eurjchem-1783	12	40	last	last	ADJ
eurjchem-1783	12	41	35	35	NUM
eurjchem-1783	12	42	years	year	NOUN
eurjchem-1783	12	43	.	.	PUNCT
eurjchem-1783	13	1	as	as	SCONJ
eurjchem-1783	13	2	the	the	DET
eurjchem-1783	13	3	first	first	ADJ
eurjchem-1783	13	4	members	member	NOUN
eurjchem-1783	13	5	,	,	PUNCT
eurjchem-1783	13	6	linezolid	linezolid	PROPN
eurjchem-1783	13	7	1a	1a	NOUN
eurjchem-1783	13	8	and	and	CCONJ
eurjchem-1783	13	9	eperezolid	eperezolid	PROPN
eurjchem-1783	13	10	1b	1b	NUM
eurjchem-1783	13	11	(	(	PUNCT
eurjchem-1783	13	12	figure	figure	NOUN
eurjchem-1783	13	13	1	1	NUM
eurjchem-1783	13	14	)	)	PUNCT
eurjchem-1783	13	15	stands	stand	VERB
eurjchem-1783	13	16	in	in	ADP
eurjchem-1783	13	17	the	the	DET
eurjchem-1783	13	18	first	first	ADJ
eurjchem-1783	13	19	line	line	NOUN
eurjchem-1783	13	20	as	as	ADP
eurjchem-1783	13	21	antibacterial	antibacterial	ADJ
eurjchem-1783	13	22	agents	agent	NOUN
eurjchem-1783	13	23	.	.	PUNCT
eurjchem-1783	14	1	recently	recently	ADV
eurjchem-1783	14	2	u.s	u.s	PROPN
eurjchem-1783	14	3	.	.	PROPN
eurjchem-1783	14	4	food	food	PROPN
eurjchem-1783	14	5	and	and	CCONJ
eurjchem-1783	14	6	drug	drug	PROPN
eurjchem-1783	14	7	administration	administration	PROPN
eurjchem-1783	14	8	(	(	PUNCT
eurjchem-1783	14	9	fda	fda	PROPN
eurjchem-1783	14	10	)	)	PUNCT
eurjchem-1783	14	11	approved	approve	VERB
eurjchem-1783	14	12	linezolid	linezolid	NOUN
eurjchem-1783	14	13	for	for	ADP
eurjchem-1783	14	14	clinical	clinical	ADJ
eurjchem-1783	14	15	use	use	NOUN
eurjchem-1783	14	16	[	[	X
eurjchem-1783	14	17	1	1	NUM
eurjchem-1783	14	18	-	-	SYM
eurjchem-1783	14	19	2	2	NUM
eurjchem-1783	14	20	]	]	PUNCT
eurjchem-1783	14	21	.	.	PUNCT
eurjchem-1783	15	1	linezolid	linezolid	PROPN
eurjchem-1783	15	2	was	be	AUX
eurjchem-1783	15	3	most	most	ADV
eurjchem-1783	15	4	potent	potent	ADJ
eurjchem-1783	15	5	in	in	ADP
eurjchem-1783	15	6	vitro	vitro	X
eurjchem-1783	15	7	activity	activity	NOUN
eurjchem-1783	15	8	against	against	ADP
eurjchem-1783	15	9	all	all	PRON
eurjchem-1783	15	10	of	of	ADP
eurjchem-1783	15	11	the	the	DET
eurjchem-1783	15	12	major	major	ADJ
eurjchem-1783	15	13	gram	gram	NOUN
eurjchem-1783	15	14	-	-	PUNCT
eurjchem-1783	15	15	positive	positive	ADJ
eurjchem-1783	15	16	bacteria	bacteria	NOUN
eurjchem-1783	15	17	[	[	X
eurjchem-1783	15	18	35	35	NUM
eurjchem-1783	15	19	]	]	PUNCT
eurjchem-1783	15	20	.	.	PUNCT
eurjchem-1783	16	1	others	other	NOUN
eurjchem-1783	16	2	members	member	NOUN
eurjchem-1783	16	3	of	of	ADP
eurjchem-1783	16	4	this	this	DET
eurjchem-1783	16	5	class	class	NOUN
eurjchem-1783	16	6	have	have	AUX
eurjchem-1783	16	7	entered	enter	VERB
eurjchem-1783	16	8	market	market	NOUN
eurjchem-1783	16	9	,	,	PUNCT
eurjchem-1783	16	10	such	such	ADJ
eurjchem-1783	16	11	as	as	ADP
eurjchem-1783	16	12	ranbezolid	ranbezolid	ADJ
eurjchem-1783	16	13	(	(	PUNCT
eurjchem-1783	16	14	rbx	rbx	NOUN
eurjchem-1783	16	15	7644	7644	NUM
eurjchem-1783	16	16	)	)	PUNCT
eurjchem-1783	16	17	,	,	PUNCT
eurjchem-1783	16	18	rivaroxaban	rivaroxaban	NOUN
eurjchem-1783	16	19	(	(	PUNCT
eurjchem-1783	16	20	bay-59	bay-59	NOUN
eurjchem-1783	16	21	-	-	PUNCT
eurjchem-1783	16	22	7939	7939	NUM
eurjchem-1783	16	23	)	)	PUNCT
eurjchem-1783	17	1	[	[	X
eurjchem-1783	17	2	6	6	NUM
eurjchem-1783	17	3	,	,	PUNCT
eurjchem-1783	17	4	7	7	NUM
eurjchem-1783	17	5	]	]	PUNCT
eurjchem-1783	17	6	,	,	PUNCT
eurjchem-1783	17	7	posizolid	posizolid	ADJ
eurjchem-1783	17	8	(	(	PUNCT
eurjchem-1783	17	9	azd	azd	PROPN
eurjchem-1783	17	10	2563	2563	NUM
eurjchem-1783	17	11	)	)	PUNCT
eurjchem-1783	18	1	[	[	X
eurjchem-1783	18	2	8	8	NUM
eurjchem-1783	18	3	]	]	PUNCT
eurjchem-1783	18	4	,	,	PUNCT
eurjchem-1783	18	5	torezolid	torezolid	INTJ
eurjchem-1783	18	6	(	(	PUNCT
eurjchem-1783	18	7	tr-701	tr-701	PROPN
eurjchem-1783	18	8	)	)	PUNCT
eurjchem-1783	19	1	[	[	X
eurjchem-1783	19	2	9	9	NUM
eurjchem-1783	19	3	]	]	PUNCT
eurjchem-1783	19	4	,	,	PUNCT
eurjchem-1783	19	5	and	and	CCONJ
eurjchem-1783	19	6	radezolid	radezolid	ADJ
eurjchem-1783	19	7	(	(	PUNCT
eurjchem-1783	19	8	rx-1741	rx-1741	NOUN
eurjchem-1783	19	9	)	)	PUNCT
eurjchem-1783	20	1	[	[	X
eurjchem-1783	20	2	10	10	NUM
eurjchem-1783	20	3	]	]	PUNCT
eurjchem-1783	20	4	.	.	PUNCT
eurjchem-1783	21	1	numerous	numerous	ADJ
eurjchem-1783	21	2	synthetic	synthetic	ADJ
eurjchem-1783	21	3	methods	method	NOUN
eurjchem-1783	21	4	are	be	AUX
eurjchem-1783	21	5	available	available	ADJ
eurjchem-1783	21	6	for	for	ADP
eurjchem-1783	21	7	the	the	DET
eurjchem-1783	21	8	preparation	preparation	NOUN
eurjchem-1783	21	9	of	of	ADP
eurjchem-1783	21	10	linezolid	linezolid	NOUN
eurjchem-1783	21	11	and	and	CCONJ
eurjchem-1783	21	12	eperezolid	eperezolid	NOUN
eurjchem-1783	21	13	since	since	SCONJ
eurjchem-1783	21	14	these	these	PRON
eurjchem-1783	21	15	are	be	AUX
eurjchem-1783	21	16	well	well	ADV
eurjchem-1783	21	17	known	know	VERB
eurjchem-1783	21	18	drugs	drug	NOUN
eurjchem-1783	21	19	in	in	ADP
eurjchem-1783	21	20	the	the	DET
eurjchem-1783	21	21	medicinal	medicinal	ADJ
eurjchem-1783	21	22	industry	industry	NOUN
eurjchem-1783	21	23	.	.	PUNCT
eurjchem-1783	22	1	one	one	NUM
eurjchem-1783	22	2	of	of	ADP
eurjchem-1783	22	3	the	the	DET
eurjchem-1783	22	4	common	common	ADJ
eurjchem-1783	22	5	synthetic	synthetic	ADJ
eurjchem-1783	22	6	strategies	strategy	NOUN
eurjchem-1783	22	7	in	in	ADP
eurjchem-1783	22	8	the	the	DET
eurjchem-1783	22	9	pharma	pharma	PROPN
eurjchem-1783	22	10	industry	industry	NOUN
eurjchem-1783	22	11	involve	involve	VERB
eurjchem-1783	22	12	conversion	conversion	NOUN
eurjchem-1783	22	13	of	of	ADP
eurjchem-1783	22	14	3fluoro-4	3fluoro-4	NOUN
eurjchem-1783	22	15	-	-	PUNCT
eurjchem-1783	22	16	morpholinobenzenamine	morpholinobenzenamine	ADJ
eurjchem-1783	22	17	(	(	PUNCT
eurjchem-1783	22	18	ar	ar	NOUN
eurjchem-1783	22	19	-	-	NOUN
eurjchem-1783	22	20	nh2	nh2	NOUN
eurjchem-1783	22	21	)	)	PUNCT
eurjchem-1783	22	22	to	to	ADP
eurjchem-1783	22	23	corresponding	corresponding	ADJ
eurjchem-1783	22	24	carbamate	carbamate	NOUN
eurjchem-1783	22	25	,	,	PUNCT
eurjchem-1783	22	26	which	which	PRON
eurjchem-1783	22	27	is	be	AUX
eurjchem-1783	22	28	deprotonated	deprotonate	VERB
eurjchem-1783	22	29	with	with	ADP
eurjchem-1783	22	30	n	n	NOUN
eurjchem-1783	22	31	-	-	PUNCT
eurjchem-1783	22	32	butyllithium	butyllithium	NOUN
eurjchem-1783	22	33	(	(	PUNCT
eurjchem-1783	22	34	nbuli	nbuli	PROPN
eurjchem-1783	22	35	)	)	PUNCT
eurjchem-1783	22	36	or	or	CCONJ
eurjchem-1783	22	37	lithiumdiisopropyl	lithiumdiisopropyl	NOUN
eurjchem-1783	22	38	amide	amide	NOUN
eurjchem-1783	22	39	(	(	PUNCT
eurjchem-1783	22	40	lda	lda	PROPN
eurjchem-1783	22	41	)	)	PUNCT
eurjchem-1783	22	42	in	in	ADP
eurjchem-1783	22	43	thf	thf	NOUN
eurjchem-1783	22	44	and	and	CCONJ
eurjchem-1783	22	45	reaction	reaction	NOUN
eurjchem-1783	22	46	with	with	ADP
eurjchem-1783	22	47	2	2	NUM
eurjchem-1783	22	48	-	-	PUNCT
eurjchem-1783	22	49	substituted	substitute	VERB
eurjchem-1783	22	50	oxirane	oxirane	NOUN
eurjchem-1783	22	51	at	at	ADP
eurjchem-1783	22	52	-78	-78	PROPN
eurjchem-1783	22	53	°	°	PROPN
eurjchem-1783	22	54	c	c	NOUN
eurjchem-1783	22	55	.	.	PUNCT
eurjchem-1783	23	1	other	other	ADJ
eurjchem-1783	23	2	methods	method	NOUN
eurjchem-1783	23	3	involve	involve	VERB
eurjchem-1783	23	4	the	the	DET
eurjchem-1783	23	5	aryl	aryl	NOUN
eurjchem-1783	23	6	carbamate	carbamate	NOUN
eurjchem-1783	23	7	was	be	AUX
eurjchem-1783	23	8	reacted	react	VERB
eurjchem-1783	23	9	with	with	ADP
eurjchem-1783	23	10	1	1	NUM
eurjchem-1783	23	11	-	-	PUNCT
eurjchem-1783	23	12	substituted	substitute	VERB
eurjchem-1783	23	13	3chloropropan-2	3chloropropan-2	NOUN
eurjchem-1783	23	14	-	-	SYM
eurjchem-1783	23	15	ol(halohydrin	ol(halohydrin	NOUN
eurjchem-1783	23	16	)	)	PUNCT
eurjchem-1783	23	17	using	use	VERB
eurjchem-1783	23	18	lithium	lithium	PROPN
eurjchem-1783	23	19	t	t	PROPN
eurjchem-1783	23	20	-	-	PUNCT
eurjchem-1783	23	21	butoxide	butoxide	NOUN
eurjchem-1783	23	22	(	(	PUNCT
eurjchem-1783	23	23	liotbu	liotbu	NOUN
eurjchem-1783	23	24	)	)	PUNCT
eurjchem-1783	23	25	or	or	CCONJ
eurjchem-1783	23	26	n	n	CCONJ
eurjchem-1783	23	27	-	-	PUNCT
eurjchem-1783	23	28	buli	buli	NOUN
eurjchem-1783	23	29	to	to	PART
eurjchem-1783	23	30	generate	generate	VERB
eurjchem-1783	23	31	(	(	PUNCT
eurjchem-1783	23	32	r)-3	r)-3	PROPN
eurjchem-1783	23	33	-	-	PUNCT
eurjchem-1783	23	34	aryl-5-(hydroxymethyl)-2	aryl-5-(hydroxymethyl)-2	NOUN
eurjchem-1783	23	35	-	-	PUNCT
eurjchem-1783	23	36	oxazolidinones	oxazolidinone	NOUN
eurjchem-1783	23	37	.	.	PUNCT
eurjchem-1783	24	1	these	these	DET
eurjchem-1783	24	2	3	3	NUM
eurjchem-1783	24	3	-	-	PUNCT
eurjchem-1783	24	4	aryl-5-(hydroxymethyl)-2	aryl-5-(hydroxymethyl)-2	NOUN
eurjchem-1783	24	5	-	-	PUNCT
eurjchem-1783	24	6	oxazolidinone	oxazolidinone	NOUN
eurjchem-1783	24	7	intermediates	intermediate	NOUN
eurjchem-1783	24	8	are	be	AUX
eurjchem-1783	24	9	castoff	castoff	NOUN
eurjchem-1783	24	10	to	to	PART
eurjchem-1783	24	11	reach	reach	VERB
eurjchem-1783	24	12	final	final	ADJ
eurjchem-1783	24	13	product	product	NOUN
eurjchem-1783	24	14	[	[	X
eurjchem-1783	24	15	11	11	NUM
eurjchem-1783	24	16	-	-	SYM
eurjchem-1783	24	17	16	16	NUM
eurjchem-1783	24	18	]	]	PUNCT
eurjchem-1783	24	19	.	.	PUNCT
eurjchem-1783	25	1	another	another	DET
eurjchem-1783	25	2	synthetic	synthetic	ADJ
eurjchem-1783	25	3	method	method	NOUN
eurjchem-1783	25	4	involves	involve	VERB
eurjchem-1783	25	5	aryl	aryl	NOUN
eurjchem-1783	25	6	isocyanate	isocyanate	NOUN
eurjchem-1783	25	7	instead	instead	ADV
eurjchem-1783	25	8	of	of	ADP
eurjchem-1783	25	9	aryl	aryl	NOUN
eurjchem-1783	25	10	carbamates	carbamate	NOUN
eurjchem-1783	25	11	.	.	PUNCT
eurjchem-1783	26	1	but	but	CCONJ
eurjchem-1783	26	2	,	,	PUNCT
eurjchem-1783	26	3	the	the	DET
eurjchem-1783	26	4	preparation	preparation	NOUN
eurjchem-1783	26	5	of	of	ADP
eurjchem-1783	26	6	aryl	aryl	NOUN
eurjchem-1783	26	7	isocyanates	isocyanate	NOUN
eurjchem-1783	26	8	is	be	AUX
eurjchem-1783	26	9	cumbersome	cumbersome	ADJ
eurjchem-1783	26	10	from	from	ADP
eurjchem-1783	26	11	multi	multi	ADJ
eurjchem-1783	26	12	-	-	ADJ
eurjchem-1783	26	13	substituted	substitute	VERB
eurjchem-1783	26	14	aryl	aryl	NOUN
eurjchem-1783	26	15	amines	amine	NOUN
eurjchem-1783	26	16	.	.	PUNCT
eurjchem-1783	27	1	moreover	moreover	ADV
eurjchem-1783	27	2	,	,	PUNCT
eurjchem-1783	27	3	while	while	SCONJ
eurjchem-1783	27	4	preparing	prepare	VERB
eurjchem-1783	27	5	aryl	aryl	NOUN
eurjchem-1783	27	6	isocyanates	isocyanate	NOUN
eurjchem-1783	27	7	a	a	DET
eurjchem-1783	27	8	major	major	ADJ
eurjchem-1783	27	9	concern	concern	NOUN
eurjchem-1783	27	10	is	be	AUX
eurjchem-1783	27	11	the	the	DET
eurjchem-1783	27	12	formation	formation	NOUN
eurjchem-1783	27	13	of	of	ADP
eurjchem-1783	27	14	corresponding	correspond	VERB
eurjchem-1783	27	15	urea	urea	NOUN
eurjchem-1783	27	16	as	as	ADP
eurjchem-1783	27	17	a	a	DET
eurjchem-1783	27	18	significant	significant	ADJ
eurjchem-1783	27	19	impurity	impurity	NOUN
eurjchem-1783	27	20	[	[	X
eurjchem-1783	27	21	17,18	17,18	NUM
eurjchem-1783	27	22	]	]	PUNCT
eurjchem-1783	27	23	.	.	PUNCT
eurjchem-1783	28	1	few	few	ADJ
eurjchem-1783	28	2	other	other	ADJ
eurjchem-1783	28	3	strategies	strategy	NOUN
eurjchem-1783	28	4	comprise	comprise	VERB
eurjchem-1783	28	5	the	the	DET
eurjchem-1783	28	6	ring	ring	NOUN
eurjchem-1783	28	7	opening	opening	NOUN
eurjchem-1783	28	8	of	of	ADP
eurjchem-1783	28	9	2	2	NUM
eurjchem-1783	28	10	-	-	PUNCT
eurjchem-1783	28	11	substituted	substitute	VERB
eurjchem-1783	28	12	oxirane	oxirane	NOUN
eurjchem-1783	28	13	using	use	VERB
eurjchem-1783	28	14	3	3	NUM
eurjchem-1783	28	15	-	-	PUNCT
eurjchem-1783	28	16	fluoro-4	fluoro-4	NUM
eurjchem-1783	28	17	-	-	PUNCT
eurjchem-1783	28	18	morpholinobenzen	morpholinobenzen	NOUN
eurjchem-1783	28	19	amine	amine	NOUN
eurjchem-1783	28	20	,	,	PUNCT
eurjchem-1783	28	21	carbonylation	carbonylation	NOUN
eurjchem-1783	28	22	followed	follow	VERB
eurjchem-1783	28	23	by	by	ADP
eurjchem-1783	28	24	further	further	ADJ
eurjchem-1783	28	25	functional	functional	ADJ
eurjchem-1783	28	26	group	group	NOUN
eurjchem-1783	28	27	transformations	transformation	NOUN
eurjchem-1783	28	28	to	to	PART
eurjchem-1783	28	29	reach	reach	VERB
eurjchem-1783	28	30	linezolid	linezolid	NOUN
eurjchem-1783	28	31	[	[	X
eurjchem-1783	28	32	19	19	NUM
eurjchem-1783	28	33	-	-	SYM
eurjchem-1783	28	34	21	21	NUM
eurjchem-1783	28	35	]	]	PUNCT
eurjchem-1783	28	36	and	and	CCONJ
eurjchem-1783	28	37	conversion	conversion	NOUN
eurjchem-1783	28	38	of	of	ADP
eurjchem-1783	28	39	(	(	PUNCT
eurjchem-1783	28	40	r)-1azido-3	r)-1azido-3	NOUN
eurjchem-1783	28	41	-	-	PUNCT
eurjchem-1783	28	42	chloropropan-2	chloropropan-2	NOUN
eurjchem-1783	28	43	-	-	PUNCT
eurjchem-1783	28	44	ol(halohydrin	ol(halohydrin	NOUN
eurjchem-1783	28	45	)	)	PUNCT
eurjchem-1783	28	46	to	to	ADP
eurjchem-1783	28	47	corresponding	correspond	VERB
eurjchem-1783	28	48	abstract	abstract	ADJ
eurjchem-1783	28	49	research	research	NOUN
eurjchem-1783	28	50	article	article	NOUN
eurjchem-1783	28	51	keywords	keyword	VERB
eurjchem-1783	28	52	european	european	PROPN
eurjchem-1783	28	53	journal	journal	PROPN
eurjchem-1783	28	54	of	of	ADP
eurjchem-1783	28	55	chemistry	chemistry	NOUN
eurjchem-1783	28	56	issn	issn	VERB
eurjchem-1783	28	57	2153	2153	NUM
eurjchem-1783	28	58	-	-	SYM
eurjchem-1783	28	59	2249	2249	NUM
eurjchem-1783	28	60	(	(	PUNCT
eurjchem-1783	28	61	print	print	NOUN
eurjchem-1783	28	62	)	)	PUNCT
eurjchem-1783	28	63	/	/	PUNCT
eurjchem-1783	28	64	issn	issn	PROPN
eurjchem-1783	28	65	2153	2153	NUM
eurjchem-1783	28	66	-	-	SYM
eurjchem-1783	28	67	2257	2257	NUM
eurjchem-1783	28	68	(	(	PUNCT
eurjchem-1783	28	69	online	online	ADJ
eurjchem-1783	28	70	)	)	PUNCT
eurjchem-1783	28	71	–	–	PUNCT
eurjchem-1783	28	72	copyright	copyright	NOUN
eurjchem-1783	28	73	©	©	PROPN
eurjchem-1783	28	74	2018	2018	NUM
eurjchem-1783	28	75	the	the	DET
eurjchem-1783	28	76	authors	author	NOUN
eurjchem-1783	28	77	–	–	PUNCT
eurjchem-1783	28	78	atlanta	atlanta	PROPN
eurjchem-1783	28	79	publishing	publishing	PROPN
eurjchem-1783	28	80	house	house	PROPN
eurjchem-1783	28	81	llc	llc	PROPN
eurjchem-1783	28	82	–	–	PUNCT
eurjchem-1783	28	83	printed	print	VERB
eurjchem-1783	28	84	in	in	ADP
eurjchem-1783	28	85	the	the	DET
eurjchem-1783	28	86	usa	usa	PROPN
eurjchem-1783	28	87	.	.	PUNCT
eurjchem-1783	29	1	this	this	DET
eurjchem-1783	29	2	work	work	NOUN
eurjchem-1783	29	3	is	be	AUX
eurjchem-1783	29	4	published	publish	VERB
eurjchem-1783	29	5	and	and	CCONJ
eurjchem-1783	29	6	licensed	license	VERB
eurjchem-1783	29	7	by	by	ADP
eurjchem-1783	29	8	atlanta	atlanta	PROPN
eurjchem-1783	29	9	publishing	publishing	PROPN
eurjchem-1783	29	10	house	house	PROPN
eurjchem-1783	29	11	llc	llc	PROPN
eurjchem-1783	29	12	–	–	PUNCT
eurjchem-1783	29	13	cc	cc	PROPN
eurjchem-1783	29	14	by	by	ADP
eurjchem-1783	29	15	nc	nc	PROPN
eurjchem-1783	29	16	–	–	PUNCT
eurjchem-1783	29	17	some	some	DET
eurjchem-1783	29	18	rights	right	NOUN
eurjchem-1783	29	19	reserved	reserve	VERB
eurjchem-1783	29	20	.	.	PUNCT
eurjchem-1783	30	1	http://dx.doi.org/10.5155/eurjchem.9.4.353-359.1783	http://dx.doi.org/10.5155/eurjchem.9.4.353-359.1783	NOUN
eurjchem-1783	30	2	http://dx.doi.org/10.5155/eurjchem.9.4.353-359.1783	http://dx.doi.org/10.5155/eurjchem.9.4.353-359.1783	PROPN
eurjchem-1783	30	3	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.9.4.353-359.1783&domain=pdf&date_stamp=2018-12-31	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.9.4.353-359.1783&domain=pdf&date_stamp=2018-12-31	NOUN
eurjchem-1783	30	4	http://www.eurjchem.com/	http://www.eurjchem.com/	NOUN
eurjchem-1783	30	5	http://dx.doi.org/10.5155/eurjchem.9.4.353-359.1783	http://dx.doi.org/10.5155/eurjchem.9.4.353-359.1783	PROPN
eurjchem-1783	30	6	mailto:ranjithsiddaraj@yahoo.co.in	mailto:ranjithsiddaraj@yahoo.co.in	PROPN
eurjchem-1783	30	7	mailto:raghu.ningegowda80@gmail.com	mailto:raghu.ningegowda80@gmail.com	PROPN
eurjchem-1783	30	8	mailto:priyabs_chem@yahoo.com	mailto:priyabs_chem@yahoo.com	X
eurjchem-1783	31	1	mailto:shivarajchemtumkur@gmail.com	mailto:shivarajchemtumkur@gmail.com	X
eurjchem-1783	31	2	mailto:nanju_chem@yahoo.com	mailto:nanju_chem@yahoo.com	PROPN
eurjchem-1783	31	3	mailto:priyabs_chem@yahoo.com	mailto:priyabs_chem@yahoo.com	PROPN
eurjchem-1783	31	4	http://www.eurjchem.com/	http://www.eurjchem.com/	PROPN
eurjchem-1783	31	5	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.9.4.353-359.1783&domain=pdf&date_stamp=2018-12-31	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.9.4.353-359.1783&domain=pdf&date_stamp=2018-12-31	PROPN
eurjchem-1783	31	6	�	�	PROPN
eurjchem-1783	31	7	354	354	NUM
eurjchem-1783	31	8	siddaraj	siddaraj	PROPN
eurjchem-1783	31	9	et	et	PROPN
eurjchem-1783	31	10	al	al	PROPN
eurjchem-1783	31	11	.	.	PUNCT
eurjchem-1783	31	12	/	/	SYM
eurjchem-1783	31	13	european	european	PROPN
eurjchem-1783	31	14	journal	journal	PROPN
eurjchem-1783	31	15	of	of	ADP
eurjchem-1783	31	16	chemistry	chemistry	NOUN
eurjchem-1783	31	17	9	9	NUM
eurjchem-1783	31	18	(	(	PUNCT
eurjchem-1783	31	19	4	4	NUM
eurjchem-1783	31	20	)	)	PUNCT
eurjchem-1783	31	21	(	(	PUNCT
eurjchem-1783	31	22	2018	2018	NUM
eurjchem-1783	31	23	)	)	PUNCT
eurjchem-1783	31	24	353	353	NUM
eurjchem-1783	31	25	-	-	SYM
eurjchem-1783	31	26	359	359	NUM
eurjchem-1783	32	1	no	no	INTJ
eurjchem-1783	32	2	n	n	ADV
eurjchem-1783	33	1	o	o	NOUN
eurjchem-1783	33	2	o	o	X
eurjchem-1783	33	3	h	h	NOUN
eurjchem-1783	33	4	n	n	ADV
eurjchem-1783	33	5	o	o	NOUN
eurjchem-1783	33	6	f	f	X
eurjchem-1783	33	7	nn	nn	PROPN
eurjchem-1783	33	8	n	n	NUM
eurjchem-1783	33	9	o	o	NOUN
eurjchem-1783	33	10	o	o	X
eurjchem-1783	33	11	h	h	NOUN
eurjchem-1783	34	1	n	n	ADV
eurjchem-1783	34	2	o	o	NOUN
eurjchem-1783	34	3	f	f	X
eurjchem-1783	34	4	o	o	X
eurjchem-1783	34	5	ho	ho	PROPN
eurjchem-1783	34	6	1a	1a	PROPN
eurjchem-1783	34	7	1b	1b	NUM
eurjchem-1783	34	8	figure	figure	NOUN
eurjchem-1783	34	9	1	1	NUM
eurjchem-1783	34	10	.	.	PUNCT
eurjchem-1783	35	1	molecular	molecular	ADJ
eurjchem-1783	35	2	structure	structure	NOUN
eurjchem-1783	35	3	of	of	ADP
eurjchem-1783	35	4	linezolid	linezolid	PROPN
eurjchem-1783	35	5	(	(	PUNCT
eurjchem-1783	35	6	1a	1a	X
eurjchem-1783	35	7	)	)	PUNCT
eurjchem-1783	35	8	and	and	CCONJ
eurjchem-1783	35	9	eperezolid	eperezolid	PROPN
eurjchem-1783	35	10	(	(	PUNCT
eurjchem-1783	35	11	1b	1b	NUM
eurjchem-1783	35	12	)	)	PUNCT
eurjchem-1783	35	13	.	.	PUNCT
eurjchem-1783	36	1	o	o	NOUN
eurjchem-1783	36	2	br	br	NOUN
eurjchem-1783	36	3	csco3	csco3	ADJ
eurjchem-1783	36	4	,	,	PUNCT
eurjchem-1783	36	5	acetonitrile	acetonitrile	NOUN
eurjchem-1783	36	6	hn	hn	NOUN
eurjchem-1783	36	7	o	o	X
eurjchem-1783	36	8	o	o	X
eurjchem-1783	36	9	ar	ar	PROPN
eurjchem-1783	36	10	n	n	ADV
eurjchem-1783	36	11	o	o	NOUN
eurjchem-1783	36	12	o	o	X
eurjchem-1783	36	13	br	br	X
eurjchem-1783	36	14	ar	ar	PROPN
eurjchem-1783	36	15	n	n	NUM
eurjchem-1783	36	16	o	o	NOUN
eurjchem-1783	36	17	o	o	NOUN
eurjchem-1783	36	18	nhac	nhac	NOUN
eurjchem-1783	36	19	aracnh2	aracnh2	NOUN
eurjchem-1783	36	20	csco3,nai	csco3,nai	ADJ
eurjchem-1783	36	21	acetonitrile	acetonitrile	NOUN
eurjchem-1783	36	22	f	f	PROPN
eurjchem-1783	36	23	f	f	PROPN
eurjchem-1783	36	24	no2	no2	PROPN
eurjchem-1783	37	1	n	n	PRON
eurjchem-1783	37	2	o	o	NOUN
eurjchem-1783	37	3	o	o	X
eurjchem-1783	37	4	br	br	NOUN
eurjchem-1783	37	5	ar	ar	PROPN
eurjchem-1783	37	6	scheme	scheme	NOUN
eurjchem-1783	37	7	1	1	NUM
eurjchem-1783	37	8	.	.	PUNCT
eurjchem-1783	38	1	synthetic	synthetic	ADJ
eurjchem-1783	38	2	strategy	strategy	NOUN
eurjchem-1783	38	3	for	for	ADP
eurjchem-1783	38	4	linezolid	linezolid	NOUN
eurjchem-1783	38	5	and	and	CCONJ
eurjchem-1783	38	6	eperezolid	eperezolid	NOUN
eurjchem-1783	38	7	.	.	PUNCT
eurjchem-1783	39	1	carbonate	carbonate	NOUN
eurjchem-1783	39	2	derivative	derivative	NOUN
eurjchem-1783	39	3	followed	follow	VERB
eurjchem-1783	39	4	by	by	ADP
eurjchem-1783	39	5	reaction	reaction	NOUN
eurjchem-1783	39	6	with	with	ADP
eurjchem-1783	39	7	ar	ar	NOUN
eurjchem-1783	39	8	-	-	NOUN
eurjchem-1783	39	9	nh2	nh2	NOUN
eurjchem-1783	39	10	to	to	PART
eurjchem-1783	39	11	accomplish	accomplish	VERB
eurjchem-1783	39	12	2	2	NUM
eurjchem-1783	39	13	-	-	PUNCT
eurjchem-1783	39	14	oxazolidinone	oxazolidinone	NOUN
eurjchem-1783	39	15	[	[	X
eurjchem-1783	39	16	22	22	NUM
eurjchem-1783	39	17	]	]	PUNCT
eurjchem-1783	39	18	.	.	PUNCT
eurjchem-1783	40	1	in	in	ADP
eurjchem-1783	40	2	addition	addition	NOUN
eurjchem-1783	40	3	,	,	PUNCT
eurjchem-1783	40	4	there	there	PRON
eurjchem-1783	40	5	are	be	VERB
eurjchem-1783	40	6	some	some	DET
eurjchem-1783	40	7	other	other	ADJ
eurjchem-1783	40	8	articles	article	NOUN
eurjchem-1783	40	9	describing	describe	VERB
eurjchem-1783	40	10	the	the	DET
eurjchem-1783	40	11	construction	construction	NOUN
eurjchem-1783	40	12	of	of	ADP
eurjchem-1783	40	13	5-(substituted	5-(substitute	VERB
eurjchem-1783	40	14	methyl)-2	methyl)-2	NOUN
eurjchem-1783	40	15	-	-	PUNCT
eurjchem-1783	40	16	oxazolidinone	oxazolidinone	NOUN
eurjchem-1783	40	17	followed	follow	VERB
eurjchem-1783	40	18	by	by	ADP
eurjchem-1783	40	19	coupling	couple	VERB
eurjchem-1783	40	20	with	with	ADP
eurjchem-1783	40	21	aryl	aryl	NOUN
eurjchem-1783	40	22	halide	halide	NOUN
eurjchem-1783	40	23	using	use	VERB
eurjchem-1783	40	24	various	various	ADJ
eurjchem-1783	40	25	reaction	reaction	NOUN
eurjchem-1783	40	26	conditions	condition	NOUN
eurjchem-1783	40	27	and	and	CCONJ
eurjchem-1783	40	28	further	further	ADJ
eurjchem-1783	40	29	transformations	transformation	NOUN
eurjchem-1783	40	30	leading	lead	VERB
eurjchem-1783	40	31	to	to	ADP
eurjchem-1783	40	32	linezolid	linezolid	PROPN
eurjchem-1783	41	1	[	[	X
eurjchem-1783	41	2	23	23	NUM
eurjchem-1783	41	3	-	-	SYM
eurjchem-1783	41	4	26	26	NUM
eurjchem-1783	41	5	]	]	PUNCT
eurjchem-1783	41	6	.	.	PUNCT
eurjchem-1783	42	1	in	in	ADP
eurjchem-1783	42	2	all	all	PRON
eurjchem-1783	42	3	of	of	ADP
eurjchem-1783	42	4	the	the	DET
eurjchem-1783	42	5	above	above	ADJ
eurjchem-1783	42	6	mentioned	mention	VERB
eurjchem-1783	42	7	methods	method	NOUN
eurjchem-1783	42	8	to	to	PART
eurjchem-1783	42	9	achieve	achieve	VERB
eurjchem-1783	42	10	the	the	DET
eurjchem-1783	42	11	key	key	ADJ
eurjchem-1783	42	12	intermediate	intermediate	ADJ
eurjchem-1783	42	13	2	2	NUM
eurjchem-1783	42	14	-	-	PUNCT
eurjchem-1783	42	15	oxazolidinone	oxazolidinone	NOUN
eurjchem-1783	42	16	ring	ring	NOUN
eurjchem-1783	42	17	highly	highly	ADV
eurjchem-1783	42	18	sensitive	sensitive	ADJ
eurjchem-1783	42	19	reagents	reagent	NOUN
eurjchem-1783	42	20	,	,	PUNCT
eurjchem-1783	42	21	and	and	CCONJ
eurjchem-1783	42	22	complex	complex	ADJ
eurjchem-1783	42	23	conversions	conversion	NOUN
eurjchem-1783	42	24	were	be	AUX
eurjchem-1783	42	25	used	use	VERB
eurjchem-1783	42	26	,	,	PUNCT
eurjchem-1783	42	27	which	which	PRON
eurjchem-1783	42	28	limit	limit	VERB
eurjchem-1783	42	29	the	the	DET
eurjchem-1783	42	30	large	large	ADJ
eurjchem-1783	42	31	-	-	PUNCT
eurjchem-1783	42	32	scale	scale	NOUN
eurjchem-1783	42	33	production	production	NOUN
eurjchem-1783	42	34	in	in	ADP
eurjchem-1783	42	35	the	the	DET
eurjchem-1783	42	36	industry	industry	NOUN
eurjchem-1783	42	37	.	.	PUNCT
eurjchem-1783	43	1	the	the	DET
eurjchem-1783	43	2	latest	late	ADJ
eurjchem-1783	43	3	analogs	analog	NOUN
eurjchem-1783	43	4	have	have	VERB
eurjchem-1783	43	5	common	common	ADJ
eurjchem-1783	43	6	functionalities	functionality	NOUN
eurjchem-1783	43	7	on	on	ADP
eurjchem-1783	43	8	the	the	DET
eurjchem-1783	43	9	c-5	c-5	NOUN
eurjchem-1783	43	10	aminomethyl	aminomethyl	PROPN
eurjchem-1783	43	11	group	group	PROPN
eurjchem-1783	43	12	,	,	PUNCT
eurjchem-1783	43	13	such	such	ADJ
eurjchem-1783	43	14	as	as	ADP
eurjchem-1783	43	15	acetamides	acetamide	NOUN
eurjchem-1783	43	16	,	,	PUNCT
eurjchem-1783	43	17	carbamates	carbamate	NOUN
eurjchem-1783	43	18	,	,	PUNCT
eurjchem-1783	43	19	ureas	urea	NOUN
eurjchem-1783	43	20	,	,	PUNCT
eurjchem-1783	43	21	thioamides	thioamide	NOUN
eurjchem-1783	43	22	,	,	PUNCT
eurjchem-1783	43	23	thiocarbamates	thiocarbamate	NOUN
eurjchem-1783	43	24	,	,	PUNCT
eurjchem-1783	43	25	and	and	CCONJ
eurjchem-1783	43	26	thioureas	thiourea	NOUN
eurjchem-1783	43	27	[	[	X
eurjchem-1783	43	28	27,28	27,28	NUM
eurjchem-1783	43	29	]	]	X
eurjchem-1783	43	30	.	.	PUNCT
eurjchem-1783	44	1	during	during	ADP
eurjchem-1783	44	2	the	the	DET
eurjchem-1783	44	3	conversion	conversion	NOUN
eurjchem-1783	44	4	of	of	ADP
eurjchem-1783	44	5	amines	amine	NOUN
eurjchem-1783	44	6	to	to	ADP
eurjchem-1783	44	7	acetamides	acetamide	NOUN
eurjchem-1783	44	8	,	,	PUNCT
eurjchem-1783	44	9	carbamates	carbamate	NOUN
eurjchem-1783	44	10	,	,	PUNCT
eurjchem-1783	44	11	ureas	urea	NOUN
eurjchem-1783	44	12	,	,	PUNCT
eurjchem-1783	44	13	thioamides	thioamide	NOUN
eurjchem-1783	44	14	,	,	PUNCT
eurjchem-1783	44	15	thiocarbamates	thiocarbamate	NOUN
eurjchem-1783	44	16	,	,	PUNCT
eurjchem-1783	44	17	and	and	CCONJ
eurjchem-1783	44	18	thioureas	thiourea	NOUN
eurjchem-1783	44	19	,	,	PUNCT
eurjchem-1783	44	20	there	there	PRON
eurjchem-1783	44	21	is	be	VERB
eurjchem-1783	44	22	a	a	DET
eurjchem-1783	44	23	higher	high	ADJ
eurjchem-1783	44	24	chance	chance	NOUN
eurjchem-1783	44	25	of	of	ADP
eurjchem-1783	44	26	obtaining	obtain	VERB
eurjchem-1783	44	27	the	the	DET
eurjchem-1783	44	28	corresponding	corresponding	ADJ
eurjchem-1783	44	29	symmetrical	symmetrical	ADJ
eurjchem-1783	44	30	derivatives	derivative	NOUN
eurjchem-1783	44	31	.	.	PUNCT
eurjchem-1783	45	1	to	to	PART
eurjchem-1783	45	2	overcome	overcome	VERB
eurjchem-1783	45	3	these	these	DET
eurjchem-1783	45	4	inadequacies	inadequacy	NOUN
eurjchem-1783	45	5	,	,	PUNCT
eurjchem-1783	45	6	we	we	PRON
eurjchem-1783	45	7	have	have	AUX
eurjchem-1783	45	8	devised	devise	VERB
eurjchem-1783	45	9	a	a	DET
eurjchem-1783	45	10	differrent	differrent	ADJ
eurjchem-1783	45	11	approach	approach	NOUN
eurjchem-1783	45	12	(	(	PUNCT
eurjchem-1783	45	13	scheme	scheme	NOUN
eurjchem-1783	45	14	1	1	NUM
eurjchem-1783	45	15	)	)	PUNCT
eurjchem-1783	45	16	for	for	ADP
eurjchem-1783	45	17	the	the	DET
eurjchem-1783	45	18	preparation	preparation	NOUN
eurjchem-1783	45	19	of	of	ADP
eurjchem-1783	45	20	the	the	DET
eurjchem-1783	45	21	linezolid	linezolid	NOUN
eurjchem-1783	45	22	and	and	CCONJ
eurjchem-1783	45	23	eperezolid	eperezolid	NOUN
eurjchem-1783	45	24	by	by	ADP
eurjchem-1783	45	25	using	use	VERB
eurjchem-1783	45	26	simple	simple	ADJ
eurjchem-1783	45	27	reagents	reagent	NOUN
eurjchem-1783	45	28	and	and	CCONJ
eurjchem-1783	45	29	ordinary	ordinary	ADJ
eurjchem-1783	45	30	reaction	reaction	NOUN
eurjchem-1783	45	31	conditions	condition	NOUN
eurjchem-1783	45	32	,	,	PUNCT
eurjchem-1783	45	33	which	which	PRON
eurjchem-1783	45	34	can	can	AUX
eurjchem-1783	45	35	be	be	AUX
eurjchem-1783	45	36	applied	apply	VERB
eurjchem-1783	45	37	to	to	ADP
eurjchem-1783	45	38	the	the	DET
eurjchem-1783	45	39	bulk	bulk	ADJ
eurjchem-1783	45	40	scale	scale	NOUN
eurjchem-1783	45	41	preparation	preparation	NOUN
eurjchem-1783	45	42	.	.	PUNCT
eurjchem-1783	46	1	2	2	X
eurjchem-1783	46	2	.	.	X
eurjchem-1783	46	3	experimental	experimental	ADJ
eurjchem-1783	46	4	2.1	2.1	NUM
eurjchem-1783	46	5	.	.	PUNCT
eurjchem-1783	47	1	instrumentation	instrumentation	NOUN
eurjchem-1783	47	2	all	all	DET
eurjchem-1783	47	3	the	the	DET
eurjchem-1783	47	4	chemicals	chemical	NOUN
eurjchem-1783	47	5	and	and	CCONJ
eurjchem-1783	47	6	solvents	solvent	NOUN
eurjchem-1783	47	7	used	use	VERB
eurjchem-1783	47	8	were	be	AUX
eurjchem-1783	47	9	procured	procure	VERB
eurjchem-1783	47	10	from	from	ADP
eurjchem-1783	47	11	merck	merck	PROPN
eurjchem-1783	47	12	and	and	CCONJ
eurjchem-1783	47	13	sigma	sigma	PROPN
eurjchem-1783	47	14	aldrich	aldrich	PROPN
eurjchem-1783	47	15	make	make	VERB
eurjchem-1783	47	16	in	in	ADP
eurjchem-1783	47	17	the	the	DET
eurjchem-1783	47	18	appropriate	appropriate	ADJ
eurjchem-1783	47	19	grade	grade	NOUN
eurjchem-1783	47	20	and	and	CCONJ
eurjchem-1783	47	21	used	use	VERB
eurjchem-1783	47	22	without	without	ADP
eurjchem-1783	47	23	further	further	ADJ
eurjchem-1783	47	24	purification	purification	NOUN
eurjchem-1783	47	25	;	;	PUNCT
eurjchem-1783	47	26	purity	purity	NOUN
eurjchem-1783	47	27	of	of	ADP
eurjchem-1783	47	28	the	the	DET
eurjchem-1783	47	29	chemicals	chemical	NOUN
eurjchem-1783	47	30	and	and	CCONJ
eurjchem-1783	47	31	solvents	solvent	NOUN
eurjchem-1783	47	32	received	receive	VERB
eurjchem-1783	47	33	was	be	AUX
eurjchem-1783	47	34	confirmed	confirm	VERB
eurjchem-1783	47	35	by	by	ADP
eurjchem-1783	47	36	thin	thin	ADJ
eurjchem-1783	47	37	layer	layer	NOUN
eurjchem-1783	47	38	chromatography	chromatography	NOUN
eurjchem-1783	47	39	.	.	PUNCT
eurjchem-1783	48	1	melting	melt	VERB
eurjchem-1783	48	2	points	point	NOUN
eurjchem-1783	48	3	were	be	AUX
eurjchem-1783	48	4	determined	determine	VERB
eurjchem-1783	48	5	in	in	ADP
eurjchem-1783	48	6	open	open	ADJ
eurjchem-1783	48	7	capillary	capillary	ADJ
eurjchem-1783	48	8	and	and	CCONJ
eurjchem-1783	48	9	are	be	AUX
eurjchem-1783	48	10	uncorrected	uncorrecte	VERB
eurjchem-1783	48	11	.	.	PUNCT
eurjchem-1783	49	1	ir	ir	PROPN
eurjchem-1783	49	2	spectra	spectra	PROPN
eurjchem-1783	49	3	were	be	AUX
eurjchem-1783	49	4	recorded	record	VERB
eurjchem-1783	49	5	on	on	ADP
eurjchem-1783	49	6	bruker	bruker	PROPN
eurjchem-1783	49	7	alpha	alpha	PROPN
eurjchem-1783	49	8	series	series	PROPN
eurjchem-1783	49	9	in	in	ADP
eurjchem-1783	49	10	kbr	kbr	PROPN
eurjchem-1783	49	11	(	(	PUNCT
eurjchem-1783	49	12	ν	ν	PROPN
eurjchem-1783	49	13	,	,	PUNCT
eurjchem-1783	49	14	cm-1	cm-1	NOUN
eurjchem-1783	49	15	)	)	PUNCT
eurjchem-1783	49	16	.	.	PUNCT
eurjchem-1783	50	1	1h	1h	NUM
eurjchem-1783	50	2	and	and	CCONJ
eurjchem-1783	50	3	13c	13c	NOUN
eurjchem-1783	50	4	nmr	nmr	NOUN
eurjchem-1783	50	5	spectra	spectra	NOUN
eurjchem-1783	50	6	were	be	AUX
eurjchem-1783	50	7	recorded	record	VERB
eurjchem-1783	50	8	on	on	ADP
eurjchem-1783	50	9	a	a	DET
eurjchem-1783	50	10	bruker	bruker	PROPN
eurjchem-1783	50	11	av400	av400	PROPN
eurjchem-1783	50	12	,	,	PUNCT
eurjchem-1783	50	13	400	400	NUM
eurjchem-1783	50	14	mhz	mhz	NOUN
eurjchem-1783	50	15	spectrometer	spectrometer	NOUN
eurjchem-1783	50	16	using	use	VERB
eurjchem-1783	50	17	tms	tms	PROPN
eurjchem-1783	50	18	as	as	ADP
eurjchem-1783	50	19	internal	internal	ADJ
eurjchem-1783	50	20	standard	standard	NOUN
eurjchem-1783	50	21	,	,	PUNCT
eurjchem-1783	50	22	lc	lc	PROPN
eurjchem-1783	50	23	-	-	PUNCT
eurjchem-1783	50	24	ms	ms	PROPN
eurjchem-1783	50	25	data	data	PROPN
eurjchem-1783	50	26	was	be	AUX
eurjchem-1783	50	27	recorded	record	VERB
eurjchem-1783	50	28	on	on	ADP
eurjchem-1783	50	29	agilent	agilent	PROPN
eurjchem-1783	50	30	waters	waters	PROPN
eurjchem-1783	50	31	,	,	PUNCT
eurjchem-1783	50	32	usa	usa	PROPN
eurjchem-1783	50	33	and	and	CCONJ
eurjchem-1783	50	34	chemical	chemical	NOUN
eurjchem-1783	50	35	shift	shift	NOUN
eurjchem-1783	50	36	values	value	NOUN
eurjchem-1783	50	37	are	be	AUX
eurjchem-1783	50	38	reported	report	VERB
eurjchem-1783	50	39	in	in	ADP
eurjchem-1783	50	40	δ	δ	PROPN
eurjchem-1783	50	41	ppm	ppm	NOUN
eurjchem-1783	50	42	.	.	PUNCT
eurjchem-1783	51	1	2.2	2.2	NUM
eurjchem-1783	51	2	.	.	PUNCT
eurjchem-1783	52	1	synthesis	synthesis	NOUN
eurjchem-1783	52	2	2.2.1	2.2.1	NUM
eurjchem-1783	52	3	.	.	PUNCT
eurjchem-1783	52	4	synthesis	synthesis	NOUN
eurjchem-1783	52	5	of	of	ADP
eurjchem-1783	52	6	4-(2	4-(2	PROPN
eurjchem-1783	52	7	-	-	PUNCT
eurjchem-1783	52	8	fluoro-4	fluoro-4	NOUN
eurjchem-1783	52	9	-	-	PUNCT
eurjchem-1783	52	10	nitrophenyl	nitrophenyl	NOUN
eurjchem-1783	52	11	)	)	PUNCT
eurjchem-1783	52	12	morpholine	morpholine	NOUN
eurjchem-1783	52	13	(	(	PUNCT
eurjchem-1783	52	14	1	1	NUM
eurjchem-1783	52	15	)	)	PUNCT
eurjchem-1783	52	16	3,4	3,4	NUM
eurjchem-1783	52	17	-	-	NUM
eurjchem-1783	52	18	difluoronitrobenzene	difluoronitrobenzene	NOUN
eurjchem-1783	52	19	(	(	PUNCT
eurjchem-1783	52	20	25	25	NUM
eurjchem-1783	52	21	g	g	NOUN
eurjchem-1783	52	22	,	,	PUNCT
eurjchem-1783	52	23	0.157	0.157	NUM
eurjchem-1783	52	24	mol	mol	NOUN
eurjchem-1783	52	25	)	)	PUNCT
eurjchem-1783	52	26	was	be	AUX
eurjchem-1783	52	27	dissolved	dissolve	VERB
eurjchem-1783	52	28	in	in	ADP
eurjchem-1783	52	29	250	250	NUM
eurjchem-1783	52	30	ml	ml	NOUN
eurjchem-1783	52	31	of	of	ADP
eurjchem-1783	52	32	dry	dry	ADJ
eurjchem-1783	52	33	thf	thf	NOUN
eurjchem-1783	52	34	(	(	PUNCT
eurjchem-1783	52	35	250	250	NUM
eurjchem-1783	52	36	ml	ml	NOUN
eurjchem-1783	52	37	)	)	PUNCT
eurjchem-1783	52	38	at	at	ADP
eurjchem-1783	52	39	room	room	NOUN
eurjchem-1783	52	40	temperature	temperature	NOUN
eurjchem-1783	52	41	,	,	PUNCT
eurjchem-1783	52	42	added	add	VERB
eurjchem-1783	52	43	morpholine	morpholine	NOUN
eurjchem-1783	52	44	(	(	PUNCT
eurjchem-1783	52	45	14.37	14.37	NUM
eurjchem-1783	52	46	g	g	NOUN
eurjchem-1783	52	47	,	,	PUNCT
eurjchem-1783	52	48	0.172	0.172	NUM
eurjchem-1783	52	49	mol	mol	NOUN
eurjchem-1783	52	50	)	)	PUNCT
eurjchem-1783	52	51	and	and	CCONJ
eurjchem-1783	52	52	triethyl	triethyl	PROPN
eurjchem-1783	52	53	amine	amine	PROPN
eurjchem-1783	52	54	(	(	PUNCT
eurjchem-1783	52	55	26.18	26.18	NUM
eurjchem-1783	52	56	ml	ml	NOUN
eurjchem-1783	52	57	,	,	PUNCT
eurjchem-1783	52	58	0.188	0.188	NUM
eurjchem-1783	52	59	mol	mol	NOUN
eurjchem-1783	52	60	)	)	PUNCT
eurjchem-1783	52	61	very	very	ADV
eurjchem-1783	52	62	slowly	slowly	ADV
eurjchem-1783	52	63	at	at	ADP
eurjchem-1783	52	64	room	room	NOUN
eurjchem-1783	52	65	temperature	temperature	NOUN
eurjchem-1783	52	66	and	and	CCONJ
eurjchem-1783	52	67	stirred	stir	VERB
eurjchem-1783	52	68	at	at	ADP
eurjchem-1783	52	69	the	the	DET
eurjchem-1783	52	70	same	same	ADJ
eurjchem-1783	52	71	for	for	ADP
eurjchem-1783	52	72	15	15	NUM
eurjchem-1783	52	73	mins	min	NOUN
eurjchem-1783	52	74	.	.	PUNCT
eurjchem-1783	53	1	reaction	reaction	NOUN
eurjchem-1783	53	2	mass	mass	PROPN
eurjchem-1783	53	3	was	be	AUX
eurjchem-1783	53	4	heated	heat	VERB
eurjchem-1783	53	5	to	to	ADP
eurjchem-1783	53	6	60	60	NUM
eurjchem-1783	53	7	°	°	NOUN
eurjchem-1783	53	8	c	c	NOUN
eurjchem-1783	53	9	for	for	ADP
eurjchem-1783	53	10	3	3	NUM
eurjchem-1783	53	11	hr	hr	NOUN
eurjchem-1783	53	12	.	.	PUNCT
eurjchem-1783	54	1	completion	completion	NOUN
eurjchem-1783	54	2	of	of	ADP
eurjchem-1783	54	3	the	the	DET
eurjchem-1783	54	4	reaction	reaction	NOUN
eurjchem-1783	54	5	was	be	AUX
eurjchem-1783	54	6	monitored	monitor	VERB
eurjchem-1783	54	7	by	by	ADP
eurjchem-1783	54	8	tlc	tlc	PROPN
eurjchem-1783	54	9	.	.	PUNCT
eurjchem-1783	55	1	after	after	ADP
eurjchem-1783	55	2	the	the	DET
eurjchem-1783	55	3	completion	completion	NOUN
eurjchem-1783	55	4	of	of	ADP
eurjchem-1783	55	5	the	the	DET
eurjchem-1783	55	6	reaction	reaction	NOUN
eurjchem-1783	55	7	,	,	PUNCT
eurjchem-1783	55	8	mass	mass	PROPN
eurjchem-1783	55	9	was	be	AUX
eurjchem-1783	55	10	added	add	VERB
eurjchem-1783	55	11	with	with	ADP
eurjchem-1783	55	12	250	250	NUM
eurjchem-1783	55	13	ml	ml	NOUN
eurjchem-1783	55	14	of	of	ADP
eurjchem-1783	55	15	water	water	NOUN
eurjchem-1783	55	16	and	and	CCONJ
eurjchem-1783	55	17	500	500	NUM
eurjchem-1783	55	18	ml	ml	NOUN
eurjchem-1783	55	19	of	of	ADP
eurjchem-1783	55	20	ethyl	ethyl	PROPN
eurjchem-1783	55	21	acetate	acetate	NOUN
eurjchem-1783	55	22	,	,	PUNCT
eurjchem-1783	55	23	organic	organic	ADJ
eurjchem-1783	55	24	layer	layer	NOUN
eurjchem-1783	55	25	was	be	AUX
eurjchem-1783	55	26	separated	separate	VERB
eurjchem-1783	55	27	,	,	PUNCT
eurjchem-1783	55	28	aqueous	aqueous	ADJ
eurjchem-1783	55	29	layer	layer	NOUN
eurjchem-1783	55	30	was	be	AUX
eurjchem-1783	55	31	extracted	extract	VERB
eurjchem-1783	55	32	with	with	ADP
eurjchem-1783	55	33	(	(	PUNCT
eurjchem-1783	55	34	2×250	2×250	NUM
eurjchem-1783	55	35	ml	ml	NOUN
eurjchem-1783	55	36	)	)	PUNCT
eurjchem-1783	55	37	,	,	PUNCT
eurjchem-1783	55	38	and	and	CCONJ
eurjchem-1783	55	39	combined	combined	ADJ
eurjchem-1783	55	40	organic	organic	ADJ
eurjchem-1783	55	41	layers	layer	NOUN
eurjchem-1783	55	42	were	be	AUX
eurjchem-1783	55	43	washed	wash	VERB
eurjchem-1783	55	44	with	with	ADP
eurjchem-1783	55	45	water	water	NOUN
eurjchem-1783	55	46	(	(	PUNCT
eurjchem-1783	55	47	2×100	2×100	NUM
eurjchem-1783	55	48	ml	ml	NOUN
eurjchem-1783	55	49	)	)	PUNCT
eurjchem-1783	55	50	,	,	PUNCT
eurjchem-1783	55	51	brine	brine	NOUN
eurjchem-1783	55	52	(	(	PUNCT
eurjchem-1783	55	53	1×100	1×100	NUM
eurjchem-1783	55	54	ml	ml	NOUN
eurjchem-1783	55	55	)	)	PUNCT
eurjchem-1783	55	56	,	,	PUNCT
eurjchem-1783	55	57	dried	dry	VERB
eurjchem-1783	55	58	over	over	ADP
eurjchem-1783	55	59	na2so4	na2so4	NOUN
eurjchem-1783	55	60	and	and	CCONJ
eurjchem-1783	55	61	concentrated	concentrate	VERB
eurjchem-1783	55	62	to	to	PART
eurjchem-1783	55	63	give	give	VERB
eurjchem-1783	55	64	crude	crude	ADJ
eurjchem-1783	55	65	product	product	NOUN
eurjchem-1783	55	66	.	.	PUNCT
eurjchem-1783	56	1	crude	crude	ADJ
eurjchem-1783	56	2	product	product	NOUN
eurjchem-1783	56	3	obtained	obtain	VERB
eurjchem-1783	56	4	was	be	AUX
eurjchem-1783	56	5	purified	purify	VERB
eurjchem-1783	56	6	by	by	ADP
eurjchem-1783	56	7	washing	wash	VERB
eurjchem-1783	56	8	it	it	PRON
eurjchem-1783	56	9	with	with	ADP
eurjchem-1783	56	10	a	a	DET
eurjchem-1783	56	11	mixture	mixture	NOUN
eurjchem-1783	56	12	of	of	ADP
eurjchem-1783	56	13	hexane	hexane	NOUN
eurjchem-1783	56	14	:	:	PUNCT
eurjchem-1783	56	15	ethyl	ethyl	PROPN
eurjchem-1783	56	16	acetate	acetate	PROPN
eurjchem-1783	56	17	(	(	PUNCT
eurjchem-1783	56	18	90:10	90:10	NUM
eurjchem-1783	56	19	,	,	PUNCT
eurjchem-1783	56	20	v	v	NOUN
eurjchem-1783	56	21	:	:	SYM
eurjchem-1783	56	22	v	v	NOUN
eurjchem-1783	56	23	)	)	PUNCT
eurjchem-1783	56	24	to	to	PART
eurjchem-1783	56	25	give	give	VERB
eurjchem-1783	56	26	pure	pure	ADJ
eurjchem-1783	56	27	product	product	NOUN
eurjchem-1783	56	28	as	as	ADP
eurjchem-1783	56	29	yellow	yellow	ADJ
eurjchem-1783	56	30	solid	solid	ADJ
eurjchem-1783	56	31	(	(	PUNCT
eurjchem-1783	56	32	scheme	scheme	NOUN
eurjchem-1783	56	33	2	2	NUM
eurjchem-1783	56	34	)	)	PUNCT
eurjchem-1783	56	35	.	.	PUNCT
eurjchem-1783	57	1	color	color	NOUN
eurjchem-1783	57	2	:	:	PUNCT
eurjchem-1783	57	3	yellow	yellow	ADJ
eurjchem-1783	57	4	.	.	PUNCT
eurjchem-1783	58	1	yield	yield	NOUN
eurjchem-1783	58	2	:	:	PUNCT
eurjchem-1783	58	3	99	99	NUM
eurjchem-1783	58	4	%	%	NOUN
eurjchem-1783	58	5	.	.	PUNCT
eurjchem-1783	59	1	m.p	m.p	PROPN
eurjchem-1783	59	2	.	.	PROPN
eurjchem-1783	59	3	:	:	PUNCT
eurjchem-1783	60	1	125	125	NUM
eurjchem-1783	60	2	-	-	SYM
eurjchem-1783	60	3	126	126	NUM
eurjchem-1783	60	4	°	°	NUM
eurjchem-1783	60	5	c	c	NOUN
eurjchem-1783	60	6	.	.	PUNCT
eurjchem-1783	61	1	1h	1h	NUM
eurjchem-1783	61	2	nmr	nmr	NOUN
eurjchem-1783	61	3	(	(	PUNCT
eurjchem-1783	61	4	400	400	NUM
eurjchem-1783	61	5	mhz	mhz	NOUN
eurjchem-1783	61	6	,	,	PUNCT
eurjchem-1783	61	7	cdcl3	cdcl3	PROPN
eurjchem-1783	61	8	,	,	PUNCT
eurjchem-1783	61	9	δ	δ	PROPN
eurjchem-1783	61	10	,	,	PUNCT
eurjchem-1783	61	11	ppm	ppm	NUM
eurjchem-1783	61	12	):	):	PUNCT
eurjchem-1783	61	13	7.96	7.96	NUM
eurjchem-1783	61	14	(	(	PUNCT
eurjchem-1783	61	15	dd	dd	PROPN
eurjchem-1783	61	16	,	,	PUNCT
eurjchem-1783	61	17	j	j	NOUN
eurjchem-1783	61	18	=	=	PROPN
eurjchem-1783	61	19	3.05	3.05	NUM
eurjchem-1783	61	20	hz	hz	NOUN
eurjchem-1783	61	21	,	,	PUNCT
eurjchem-1783	61	22	1h	1h	NUM
eurjchem-1783	61	23	,	,	PUNCT
eurjchem-1783	61	24	ar	ar	NOUN
eurjchem-1783	61	25	-	-	NOUN
eurjchem-1783	61	26	h	h	NOUN
eurjchem-1783	61	27	)	)	PUNCT
eurjchem-1783	61	28	,	,	PUNCT
eurjchem-1783	61	29	7.86	7.86	NUM
eurjchem-1783	61	30	(	(	PUNCT
eurjchem-1783	61	31	dd	dd	PROPN
eurjchem-1783	61	32	,	,	PUNCT
eurjchem-1783	61	33	j	j	NOUN
eurjchem-1783	62	1	=	=	SYM
eurjchem-1783	62	2	3.55	3.55	NUM
eurjchem-1783	62	3	hz	hz	NOUN
eurjchem-1783	62	4	,	,	PUNCT
eurjchem-1783	62	5	1h	1h	NUM
eurjchem-1783	62	6	,	,	PUNCT
eurjchem-1783	62	7	ar	ar	NOUN
eurjchem-1783	62	8	-	-	NOUN
eurjchem-1783	62	9	h	h	NOUN
eurjchem-1783	62	10	)	)	PUNCT
eurjchem-1783	62	11	,	,	PUNCT
eurjchem-1783	62	12	6.87	6.87	NUM
eurjchem-1783	62	13	(	(	PUNCT
eurjchem-1783	62	14	dd	dd	PROPN
eurjchem-1783	62	15	,	,	PUNCT
eurjchem-1783	62	16	j	j	PROPN
eurjchem-1783	62	17	=	=	SYM
eurjchem-1783	62	18	4.50	4.50	NUM
eurjchem-1783	62	19	,	,	PUNCT
eurjchem-1783	62	20	1h	1h	NUM
eurjchem-1783	62	21	,	,	PUNCT
eurjchem-1783	62	22	ar	ar	NOUN
eurjchem-1783	62	23	-	-	NOUN
eurjchem-1783	62	24	h	h	NOUN
eurjchem-1783	62	25	)	)	PUNCT
eurjchem-1783	62	26	,	,	PUNCT
eurjchem-1783	62	27	3.84	3.84	NUM
eurjchem-1783	62	28	(	(	PUNCT
eurjchem-1783	62	29	t	t	PROPN
eurjchem-1783	62	30	,	,	PUNCT
eurjchem-1783	62	31	j	j	PROPN
eurjchem-1783	63	1	=	=	SYM
eurjchem-1783	63	2	8	8	NUM
eurjchem-1783	63	3	hz	hz	NOUN
eurjchem-1783	63	4	,	,	PUNCT
eurjchem-1783	63	5	4h	4h	NOUN
eurjchem-1783	63	6	,	,	PUNCT
eurjchem-1783	63	7	morpholine	morpholine	NOUN
eurjchem-1783	63	8	-	-	PUNCT
eurjchem-1783	63	9	ch2	ch2	NOUN
eurjchem-1783	63	10	)	)	PUNCT
eurjchem-1783	63	11	,	,	PUNCT
eurjchem-1783	63	12	3.27	3.27	NUM
eurjchem-1783	63	13	(	(	PUNCT
eurjchem-1783	63	14	t	t	PROPN
eurjchem-1783	63	15	,	,	PUNCT
eurjchem-1783	63	16	j	j	PROPN
eurjchem-1783	64	1	=	=	SYM
eurjchem-1783	64	2	8	8	NUM
eurjchem-1783	64	3	hz	hz	NOUN
eurjchem-1783	64	4	,	,	PUNCT
eurjchem-1783	64	5	4h	4h	NOUN
eurjchem-1783	64	6	,	,	PUNCT
eurjchem-1783	64	7	morpholine	morpholine	NOUN
eurjchem-1783	64	8	-	-	PUNCT
eurjchem-1783	64	9	ch2	ch2	NOUN
eurjchem-1783	64	10	)	)	PUNCT
eurjchem-1783	64	11	.	.	PUNCT
eurjchem-1783	65	1	13c	13c	NOUN
eurjchem-1783	65	2	nmr	nmr	NOUN
eurjchem-1783	65	3	(	(	PUNCT
eurjchem-1783	65	4	100	100	NUM
eurjchem-1783	65	5	mhz	mhz	NOUN
eurjchem-1783	65	6	,	,	PUNCT
eurjchem-1783	65	7	cdcl3	cdcl3	PROPN
eurjchem-1783	65	8	,	,	PUNCT
eurjchem-1783	65	9	δ	δ	PROPN
eurjchem-1783	65	10	,	,	PUNCT
eurjchem-1783	65	11	ppm	ppm	NUM
eurjchem-1783	65	12	):	):	PUNCT
eurjchem-1783	65	13	155.6	155.6	NUM
eurjchem-1783	65	14	(	(	PUNCT
eurjchem-1783	65	15	1c	1c	NOUN
eurjchem-1783	65	16	,	,	PUNCT
eurjchem-1783	65	17	ar	ar	NOUN
eurjchem-1783	65	18	-	-	NOUN
eurjchem-1783	65	19	c	c	NOUN
eurjchem-1783	65	20	)	)	PUNCT
eurjchem-1783	65	21	,	,	PUNCT
eurjchem-1783	65	22	150.6	150.6	NUM
eurjchem-1783	65	23	(	(	PUNCT
eurjchem-1783	65	24	1c	1c	NOUN
eurjchem-1783	65	25	,	,	PUNCT
eurjchem-1783	65	26	arc	arc	NOUN
eurjchem-1783	65	27	)	)	PUNCT
eurjchem-1783	65	28	,	,	PUNCT
eurjchem-1783	65	29	145.5	145.5	NUM
eurjchem-1783	65	30	(	(	PUNCT
eurjchem-1783	65	31	1c	1c	NOUN
eurjchem-1783	65	32	,	,	PUNCT
eurjchem-1783	65	33	ar	ar	NOUN
eurjchem-1783	65	34	-	-	NOUN
eurjchem-1783	65	35	c	c	NOUN
eurjchem-1783	65	36	)	)	PUNCT
eurjchem-1783	65	37	,	,	PUNCT
eurjchem-1783	65	38	121.0	121.0	NUM
eurjchem-1783	65	39	(	(	PUNCT
eurjchem-1783	65	40	1c	1c	X
eurjchem-1783	65	41	,	,	PUNCT
eurjchem-1783	65	42	ar	ar	NOUN
eurjchem-1783	65	43	-	-	NOUN
eurjchem-1783	65	44	c	c	NOUN
eurjchem-1783	65	45	)	)	PUNCT
eurjchem-1783	65	46	,	,	PUNCT
eurjchem-1783	65	47	120.9	120.9	NUM
eurjchem-1783	65	48	(	(	PUNCT
eurjchem-1783	65	49	1c	1c	NOUN
eurjchem-1783	65	50	,	,	PUNCT
eurjchem-1783	65	51	ar	ar	NOUN
eurjchem-1783	65	52	-	-	NOUN
eurjchem-1783	65	53	c	c	NOUN
eurjchem-1783	65	54	)	)	PUNCT
eurjchem-1783	65	55	,	,	PUNCT
eurjchem-1783	65	56	112.8	112.8	NUM
eurjchem-1783	65	57	(	(	PUNCT
eurjchem-1783	65	58	1c	1c	NOUN
eurjchem-1783	65	59	,	,	PUNCT
eurjchem-1783	65	60	ar	ar	NOUN
eurjchem-1783	65	61	-	-	NOUN
eurjchem-1783	65	62	c	c	NOUN
eurjchem-1783	65	63	)	)	PUNCT
eurjchem-1783	65	64	,	,	PUNCT
eurjchem-1783	65	65	66.5	66.5	NUM
eurjchem-1783	65	66	(	(	PUNCT
eurjchem-1783	65	67	2c	2c	NOUN
eurjchem-1783	65	68	,	,	PUNCT
eurjchem-1783	65	69	ch2	ch2	PROPN
eurjchem-1783	65	70	)	)	PUNCT
eurjchem-1783	65	71	,	,	PUNCT
eurjchem-1783	65	72	49.8	49.8	NUM
eurjchem-1783	65	73	(	(	PUNCT
eurjchem-1783	65	74	2c	2c	NOUN
eurjchem-1783	65	75	,	,	PUNCT
eurjchem-1783	65	76	ch2	ch2	PROPN
eurjchem-1783	65	77	)	)	PUNCT
eurjchem-1783	65	78	.	.	PUNCT
eurjchem-1783	66	1	ms	ms	NOUN
eurjchem-1783	66	2	(	(	PUNCT
eurjchem-1783	66	3	m	m	PROPN
eurjchem-1783	66	4	/	/	SYM
eurjchem-1783	66	5	z	z	NOUN
eurjchem-1783	66	6	):	):	PUNCT
eurjchem-1783	66	7	227.1	227.1	NUM
eurjchem-1783	66	8	(	(	PUNCT
eurjchem-1783	66	9	m+	m+	NUM
eurjchem-1783	66	10	)	)	PUNCT
eurjchem-1783	66	11	.	.	PUNCT
eurjchem-1783	67	1	anal	anal	PROPN
eurjchem-1783	67	2	.	.	PUNCT
eurjchem-1783	67	3	calcd	calcd	NOUN
eurjchem-1783	67	4	.	.	PUNCT
eurjchem-1783	68	1	for	for	ADP
eurjchem-1783	68	2	c10h11fn2o3	c10h11fn2o3	NOUN
eurjchem-1783	68	3	:	:	PUNCT
eurjchem-1783	68	4	c	c	X
eurjchem-1783	68	5	,	,	PUNCT
eurjchem-1783	68	6	53.10	53.10	NUM
eurjchem-1783	68	7	;	;	PUNCT
eurjchem-1783	68	8	h	h	NOUN
eurjchem-1783	68	9	,	,	PUNCT
eurjchem-1783	68	10	4.90	4.90	NUM
eurjchem-1783	68	11	;	;	PUNCT
eurjchem-1783	68	12	n	n	CCONJ
eurjchem-1783	68	13	,	,	PUNCT
eurjchem-1783	68	14	12.38	12.38	NUM
eurjchem-1783	68	15	.	.	PUNCT
eurjchem-1783	68	16	found	find	VERB
eurjchem-1783	68	17	:	:	PUNCT
eurjchem-1783	69	1	c	c	X
eurjchem-1783	69	2	,	,	PUNCT
eurjchem-1783	69	3	53.08	53.08	NUM
eurjchem-1783	69	4	;	;	PUNCT
eurjchem-1783	69	5	h	h	NOUN
eurjchem-1783	69	6	,	,	PUNCT
eurjchem-1783	69	7	4.95	4.95	NUM
eurjchem-1783	69	8	;	;	PUNCT
eurjchem-1783	69	9	n	n	CCONJ
eurjchem-1783	69	10	,	,	PUNCT
eurjchem-1783	69	11	12.14	12.14	NUM
eurjchem-1783	69	12	%	%	NOUN
eurjchem-1783	69	13	.	.	PUNCT
eurjchem-1783	70	1	2.2.2	2.2.2	X
eurjchem-1783	70	2	.	.	X
eurjchem-1783	70	3	synthesis	synthesis	NOUN
eurjchem-1783	70	4	3	3	NUM
eurjchem-1783	70	5	-	-	PUNCT
eurjchem-1783	70	6	fluoro-4	fluoro-4	NOUN
eurjchem-1783	70	7	-	-	PUNCT
eurjchem-1783	70	8	morpholinoaniline	morpholinoaniline	NOUN
eurjchem-1783	70	9	(	(	PUNCT
eurjchem-1783	70	10	2	2	NUM
eurjchem-1783	70	11	)	)	PUNCT
eurjchem-1783	70	12	4-(2	4-(2	PROPN
eurjchem-1783	70	13	-	-	PUNCT
eurjchem-1783	70	14	fluoro-4	fluoro-4	NOUN
eurjchem-1783	70	15	-	-	PUNCT
eurjchem-1783	70	16	nitrophenyl	nitrophenyl	NOUN
eurjchem-1783	70	17	)	)	PUNCT
eurjchem-1783	70	18	morpholine	morpholine	NOUN
eurjchem-1783	70	19	(	(	PUNCT
eurjchem-1783	70	20	25	25	NUM
eurjchem-1783	70	21	g	g	NOUN
eurjchem-1783	70	22	,	,	PUNCT
eurjchem-1783	70	23	0.11	0.11	NUM
eurjchem-1783	70	24	mol	mol	NOUN
eurjchem-1783	70	25	)	)	PUNCT
eurjchem-1783	70	26	was	be	AUX
eurjchem-1783	70	27	dissolved	dissolve	VERB
eurjchem-1783	70	28	in	in	ADP
eurjchem-1783	70	29	ethanol	ethanol	NOUN
eurjchem-1783	70	30	(	(	PUNCT
eurjchem-1783	70	31	200	200	NUM
eurjchem-1783	70	32	ml	ml	NOUN
eurjchem-1783	70	33	)	)	PUNCT
eurjchem-1783	70	34	in	in	ADP
eurjchem-1783	70	35	a	a	DET
eurjchem-1783	70	36	three	three	NUM
eurjchem-1783	70	37	necked	neck	VERB
eurjchem-1783	70	38	round	round	ADJ
eurjchem-1783	70	39	bottom	bottom	ADJ
eurjchem-1783	70	40	flask	flask	NOUN
eurjchem-1783	70	41	fitted	fit	VERB
eurjchem-1783	70	42	with	with	ADP
eurjchem-1783	70	43	the	the	DET
eurjchem-1783	70	44	condenser	condenser	NOUN
eurjchem-1783	70	45	and	and	CCONJ
eurjchem-1783	70	46	cooled	cool	VERB
eurjchem-1783	70	47	to	to	ADP
eurjchem-1783	70	48	-10	-10	PUNCT
eurjchem-1783	70	49	°	°	PRON
eurjchem-1783	70	50	c	c	NOUN
eurjchem-1783	70	51	.	.	PUNCT
eurjchem-1783	71	1	raney	raney	PROPN
eurjchem-1783	71	2	nickel	nickel	NOUN
eurjchem-1783	71	3	catalyst	catalyst	NOUN
eurjchem-1783	71	4	(	(	PUNCT
eurjchem-1783	71	5	1.25	1.25	NUM
eurjchem-1783	71	6	g	g	NOUN
eurjchem-1783	71	7	)	)	PUNCT
eurjchem-1783	71	8	was	be	AUX
eurjchem-1783	71	9	suspended	suspend	VERB
eurjchem-1783	71	10	in	in	ADP
eurjchem-1783	71	11	ethanol	ethanol	NOUN
eurjchem-1783	71	12	(	(	PUNCT
eurjchem-1783	71	13	50	50	NUM
eurjchem-1783	71	14	ml	ml	NOUN
eurjchem-1783	71	15	)	)	PUNCT
eurjchem-1783	71	16	was	be	AUX
eurjchem-1783	71	17	introduced	introduce	VERB
eurjchem-1783	71	18	in	in	ADP
eurjchem-1783	71	19	to	to	ADP
eurjchem-1783	71	20	the	the	DET
eurjchem-1783	71	21	flask	flask	NOUN
eurjchem-1783	71	22	at	at	ADP
eurjchem-1783	71	23	-10	-10	PUNCT
eurjchem-1783	71	24	°	°	PRON
eurjchem-1783	71	25	c	c	NOUN
eurjchem-1783	71	26	.	.	PUNCT
eurjchem-1783	71	27	hydrazine	hydrazine	NOUN
eurjchem-1783	71	28	hydrate	hydrate	NOUN
eurjchem-1783	71	29	(	(	PUNCT
eurjchem-1783	71	30	5.73	5.73	NUM
eurjchem-1783	71	31	ml	ml	NOUN
eurjchem-1783	71	32	,	,	PUNCT
eurjchem-1783	71	33	0.184	0.184	NUM
eurjchem-1783	71	34	mol	mol	NOUN
eurjchem-1783	71	35	)	)	PUNCT
eurjchem-1783	71	36	was	be	AUX
eurjchem-1783	71	37	added	add	VERB
eurjchem-1783	71	38	to	to	ADP
eurjchem-1783	71	39	the	the	DET
eurjchem-1783	71	40	flask	flask	NOUN
eurjchem-1783	71	41	through	through	ADP
eurjchem-1783	71	42	the	the	DET
eurjchem-1783	71	43	syringe	syringe	NOUN
eurjchem-1783	71	44	by	by	ADP
eurjchem-1783	71	45	maintaining	maintain	VERB
eurjchem-1783	71	46	the	the	DET
eurjchem-1783	71	47	temperature	temperature	NOUN
eurjchem-1783	71	48	below	below	ADP
eurjchem-1783	71	49	0	0	NUM
eurjchem-1783	72	1	°	°	ADP
eurjchem-1783	72	2	c	c	NOUN
eurjchem-1783	72	3	.	.	PUNCT
eurjchem-1783	73	1	reaction	reaction	NOUN
eurjchem-1783	73	2	was	be	AUX
eurjchem-1783	73	3	stirred	stir	VERB
eurjchem-1783	73	4	at	at	ADP
eurjchem-1783	73	5	room	room	NOUN
eurjchem-1783	73	6	temperature	temperature	NOUN
eurjchem-1783	73	7	for	for	ADP
eurjchem-1783	73	8	30	30	NUM
eurjchem-1783	73	9	mins	min	NOUN
eurjchem-1783	73	10	and	and	CCONJ
eurjchem-1783	73	11	the	the	DET
eurjchem-1783	73	12	completion	completion	NOUN
eurjchem-1783	73	13	of	of	ADP
eurjchem-1783	73	14	the	the	DET
eurjchem-1783	73	15	reaction	reaction	NOUN
eurjchem-1783	73	16	was	be	AUX
eurjchem-1783	73	17	monitored	monitor	VERB
eurjchem-1783	73	18	by	by	ADP
eurjchem-1783	73	19	tlc	tlc	PROPN
eurjchem-1783	73	20	.	.	PUNCT
eurjchem-1783	74	1	after	after	ADP
eurjchem-1783	74	2	the	the	DET
eurjchem-1783	74	3	completion	completion	NOUN
eurjchem-1783	74	4	the	the	DET
eurjchem-1783	74	5	reaction	reaction	NOUN
eurjchem-1783	74	6	mass	mass	NOUN
eurjchem-1783	74	7	was	be	AUX
eurjchem-1783	74	8	filtered	filter	VERB
eurjchem-1783	74	9	through	through	ADP
eurjchem-1783	74	10	the	the	DET
eurjchem-1783	74	11	celite	celite	ADJ
eurjchem-1783	74	12	bed	bed	NOUN
eurjchem-1783	74	13	to	to	PART
eurjchem-1783	74	14	remove	remove	VERB
eurjchem-1783	74	15	raney	raney	NOUN
eurjchem-1783	74	16	nickel	nickel	NOUN
eurjchem-1783	74	17	,	,	PUNCT
eurjchem-1783	74	18	washed	wash	VERB
eurjchem-1783	74	19	with	with	ADP
eurjchem-1783	74	20	ethanol	ethanol	NOUN
eurjchem-1783	74	21	(	(	PUNCT
eurjchem-1783	74	22	2×50	2×50	NUM
eurjchem-1783	74	23	ml	ml	NOUN
eurjchem-1783	74	24	)	)	PUNCT
eurjchem-1783	74	25	,	,	PUNCT
eurjchem-1783	74	26	concentrated	concentrate	VERB
eurjchem-1783	74	27	to	to	PART
eurjchem-1783	74	28	give	give	VERB
eurjchem-1783	74	29	crude	crude	ADJ
eurjchem-1783	74	30	product	product	NOUN
eurjchem-1783	74	31	as	as	ADP
eurjchem-1783	74	32	brown	brown	ADJ
eurjchem-1783	74	33	solid	solid	ADJ
eurjchem-1783	74	34	(	(	PUNCT
eurjchem-1783	74	35	scheme	scheme	NOUN
eurjchem-1783	74	36	2	2	NUM
eurjchem-1783	74	37	)	)	PUNCT
eurjchem-1783	74	38	.	.	PUNCT
eurjchem-1783	75	1	color	color	NOUN
eurjchem-1783	75	2	:	:	PUNCT
eurjchem-1783	75	3	brown	brown	ADJ
eurjchem-1783	75	4	.	.	PUNCT
eurjchem-1783	76	1	yield	yield	NOUN
eurjchem-1783	76	2	:	:	PUNCT
eurjchem-1783	76	3	92	92	NUM
eurjchem-1783	76	4	%	%	NOUN
eurjchem-1783	76	5	.	.	PUNCT
eurjchem-1783	77	1	m.p	m.p	PROPN
eurjchem-1783	77	2	.	.	PROPN
eurjchem-1783	77	3	:	:	PUNCT
eurjchem-1783	78	1	134	134	NUM
eurjchem-1783	78	2	-	-	SYM
eurjchem-1783	78	3	136	136	NUM
eurjchem-1783	78	4	°	°	NUM
eurjchem-1783	78	5	c	c	NOUN
eurjchem-1783	78	6	.	.	PUNCT
eurjchem-1783	79	1	1h	1h	NUM
eurjchem-1783	79	2	nmr	nmr	NOUN
eurjchem-1783	79	3	(	(	PUNCT
eurjchem-1783	79	4	400	400	NUM
eurjchem-1783	79	5	mhz	mhz	NOUN
eurjchem-1783	79	6	,	,	PUNCT
eurjchem-1783	79	7	cdcl3	cdcl3	PROPN
eurjchem-1783	79	8	,	,	PUNCT
eurjchem-1783	79	9	δ	δ	PROPN
eurjchem-1783	79	10	,	,	PUNCT
eurjchem-1783	79	11	ppm	ppm	NUM
eurjchem-1783	79	12	):	):	PUNCT
eurjchem-1783	79	13	6.85	6.85	NUM
eurjchem-1783	79	14	(	(	PUNCT
eurjchem-1783	79	15	d	d	NOUN
eurjchem-1783	79	16	,	,	PUNCT
eurjchem-1783	79	17	j	j	PROPN
eurjchem-1783	79	18	=	=	SYM
eurjchem-1783	79	19	4	4	NUM
eurjchem-1783	79	20	hz	hz	NOUN
eurjchem-1783	79	21	,	,	PUNCT
eurjchem-1783	79	22	1h	1h	NUM
eurjchem-1783	79	23	,	,	PUNCT
eurjchem-1783	79	24	ar	ar	NOUN
eurjchem-1783	79	25	-	-	NOUN
eurjchem-1783	79	26	h	h	NOUN
eurjchem-1783	79	27	)	)	PUNCT
eurjchem-1783	79	28	,	,	PUNCT
eurjchem-1783	79	29	6.73	6.73	NUM
eurjchem-1783	79	30	(	(	PUNCT
eurjchem-1783	79	31	dd	dd	PROPN
eurjchem-1783	79	32	,	,	PUNCT
eurjchem-1783	79	33	j	j	NOUN
eurjchem-1783	79	34	=	=	SYM
eurjchem-1783	79	35	4.2	4.2	NUM
eurjchem-1783	79	36	hz	hz	NOUN
eurjchem-1783	79	37	,	,	PUNCT
eurjchem-1783	79	38	1h	1h	NUM
eurjchem-1783	79	39	,	,	PUNCT
eurjchem-1783	79	40	ar	ar	NOUN
eurjchem-1783	79	41	-	-	NOUN
eurjchem-1783	79	42	h	h	NOUN
eurjchem-1783	79	43	)	)	PUNCT
eurjchem-1783	79	44	,	,	PUNCT
eurjchem-1783	79	45	6.52	6.52	NUM
eurjchem-1783	79	46	(	(	PUNCT
eurjchem-1783	79	47	dd	dd	NOUN
eurjchem-1783	79	48	,	,	PUNCT
eurjchem-1783	79	49	j	j	PROPN
eurjchem-1783	80	1	=	=	SYM
eurjchem-1783	80	2	6.2	6.2	NUM
eurjchem-1783	80	3	hz	hz	NOUN
eurjchem-1783	80	4	,	,	PUNCT
eurjchem-1783	80	5	1h	1h	NUM
eurjchem-1783	80	6	,	,	PUNCT
eurjchem-1783	80	7	ar	ar	NOUN
eurjchem-1783	80	8	-	-	NOUN
eurjchem-1783	80	9	h	h	NOUN
eurjchem-1783	80	10	)	)	PUNCT
eurjchem-1783	80	11	,	,	PUNCT
eurjchem-1783	80	12	3.81	3.81	NUM
eurjchem-1783	80	13	(	(	PUNCT
eurjchem-1783	80	14	t	t	PROPN
eurjchem-1783	80	15	,	,	PUNCT
eurjchem-1783	80	16	j	j	PROPN
eurjchem-1783	81	1	=	=	SYM
eurjchem-1783	81	2	3	3	NUM
eurjchem-1783	81	3	hz	hz	NOUN
eurjchem-1783	81	4	,	,	PUNCT
eurjchem-1783	81	5	4h	4h	NOUN
eurjchem-1783	81	6	,	,	PUNCT
eurjchem-1783	81	7	morpholine	morpholine	NOUN
eurjchem-1783	81	8	-	-	PUNCT
eurjchem-1783	81	9	ch2	ch2	NOUN
eurjchem-1783	81	10	)	)	PUNCT
eurjchem-1783	81	11	,	,	PUNCT
eurjchem-1783	81	12	3.35	3.35	NUM
eurjchem-1783	81	13	(	(	PUNCT
eurjchem-1783	81	14	s	s	PROPN
eurjchem-1783	81	15	,	,	PUNCT
eurjchem-1783	81	16	2h	2h	NUM
eurjchem-1783	81	17	,	,	PUNCT
eurjchem-1783	81	18	nh2	nh2	PROPN
eurjchem-1783	81	19	)	)	PUNCT
eurjchem-1783	81	20	,	,	PUNCT
eurjchem-1783	81	21	2.90	2.90	NUM
eurjchem-1783	81	22	(	(	PUNCT
eurjchem-1783	81	23	t	t	PROPN
eurjchem-1783	81	24	,	,	PUNCT
eurjchem-1783	81	25	j	j	PROPN
eurjchem-1783	81	26	=	=	SYM
eurjchem-1783	81	27	3	3	NUM
eurjchem-1783	81	28	hz	hz	NOUN
eurjchem-1783	81	29	,	,	PUNCT
eurjchem-1783	81	30	4h	4h	NOUN
eurjchem-1783	81	31	,	,	PUNCT
eurjchem-1783	81	32	morpholine	morpholine	NOUN
eurjchem-1783	81	33	-	-	PUNCT
eurjchem-1783	81	34	ch2	ch2	NOUN
eurjchem-1783	81	35	)	)	PUNCT
eurjchem-1783	81	36	.	.	PUNCT
eurjchem-1783	82	1	13c	13c	NOUN
eurjchem-1783	82	2	nmr	nmr	NOUN
eurjchem-1783	82	3	(	(	PUNCT
eurjchem-1783	82	4	100	100	NUM
eurjchem-1783	82	5	mhz	mhz	NOUN
eurjchem-1783	82	6	,	,	PUNCT
eurjchem-1783	82	7	cdcl3	cdcl3	PROPN
eurjchem-1783	82	8	,	,	PUNCT
eurjchem-1783	82	9	δ	δ	PROPN
eurjchem-1783	82	10	,	,	PUNCT
eurjchem-1783	82	11	ppm	ppm	NUM
eurjchem-1783	82	12	):	):	PUNCT
eurjchem-1783	82	13	143.01	143.01	NUM
eurjchem-1783	82	14	(	(	PUNCT
eurjchem-1783	82	15	1c	1c	X
eurjchem-1783	82	16	,	,	PUNCT
eurjchem-1783	82	17	ar	ar	NOUN
eurjchem-1783	82	18	-	-	NOUN
eurjchem-1783	82	19	c	c	NOUN
eurjchem-1783	82	20	)	)	PUNCT
eurjchem-1783	82	21	,	,	PUNCT
eurjchem-1783	82	22	140.63	140.63	NUM
eurjchem-1783	82	23	(	(	PUNCT
eurjchem-1783	82	24	1c	1c	NOUN
eurjchem-1783	82	25	,	,	PUNCT
eurjchem-1783	82	26	ar	ar	NOUN
eurjchem-1783	82	27	-	-	NOUN
eurjchem-1783	82	28	c	c	NOUN
eurjchem-1783	82	29	)	)	PUNCT
eurjchem-1783	82	30	,	,	PUNCT
eurjchem-1783	82	31	129.78	129.78	NUM
eurjchem-1783	82	32	(	(	PUNCT
eurjchem-1783	82	33	1c	1c	NOUN
eurjchem-1783	82	34	,	,	PUNCT
eurjchem-1783	82	35	ar	ar	NOUN
eurjchem-1783	82	36	-	-	NOUN
eurjchem-1783	82	37	c	c	NOUN
eurjchem-1783	82	38	)	)	PUNCT
eurjchem-1783	82	39	,	,	PUNCT
eurjchem-1783	82	40	121.22	121.22	NUM
eurjchem-1783	82	41	(	(	PUNCT
eurjchem-1783	82	42	1c	1c	NOUN
eurjchem-1783	82	43	,	,	PUNCT
eurjchem-1783	82	44	ar	ar	NOUN
eurjchem-1783	82	45	-	-	NOUN
eurjchem-1783	82	46	c	c	NOUN
eurjchem-1783	82	47	)	)	PUNCT
eurjchem-1783	82	48	,	,	PUNCT
eurjchem-1783	82	49	117.09	117.09	NUM
eurjchem-1783	82	50	(	(	PUNCT
eurjchem-1783	82	51	1c	1c	NOUN
eurjchem-1783	82	52	,	,	PUNCT
eurjchem-1783	82	53	ar	ar	NOUN
eurjchem-1783	82	54	-	-	NOUN
eurjchem-1783	82	55	c	c	NOUN
eurjchem-1783	82	56	)	)	PUNCT
eurjchem-1783	82	57	,	,	PUNCT
eurjchem-1783	82	58	114.14	114.14	NUM
eurjchem-1783	82	59	(	(	PUNCT
eurjchem-1783	82	60	1c	1c	NOUN
eurjchem-1783	82	61	,	,	PUNCT
eurjchem-1783	82	62	ar	ar	NOUN
eurjchem-1783	82	63	-	-	NOUN
eurjchem-1783	82	64	c	c	NOUN
eurjchem-1783	82	65	)	)	PUNCT
eurjchem-1783	82	66	,	,	PUNCT
eurjchem-1783	82	67	67.23	67.23	NUM
eurjchem-1783	82	68	(	(	PUNCT
eurjchem-1783	82	69	2c	2c	NOUN
eurjchem-1783	82	70	,	,	PUNCT
eurjchem-1783	82	71	ch2	ch2	PROPN
eurjchem-1783	82	72	)	)	PUNCT
eurjchem-1783	82	73	,	,	PUNCT
eurjchem-1783	82	74	52.18	52.18	NUM
eurjchem-1783	82	75	(	(	PUNCT
eurjchem-1783	82	76	2c	2c	NOUN
eurjchem-1783	82	77	,	,	PUNCT
eurjchem-1783	82	78	ch2	ch2	PROPN
eurjchem-1783	82	79	)	)	PUNCT
eurjchem-1783	82	80	.	.	PUNCT
eurjchem-1783	83	1	ms	ms	NOUN
eurjchem-1783	83	2	(	(	PUNCT
eurjchem-1783	83	3	m	m	PROPN
eurjchem-1783	83	4	/	/	SYM
eurjchem-1783	83	5	z	z	NOUN
eurjchem-1783	83	6	):	):	PUNCT
eurjchem-1783	83	7	197.2	197.2	NUM
eurjchem-1783	83	8	(	(	PUNCT
eurjchem-1783	83	9	m+	m+	NUM
eurjchem-1783	83	10	)	)	PUNCT
eurjchem-1783	83	11	.	.	PUNCT
eurjchem-1783	84	1	anal	anal	PROPN
eurjchem-1783	84	2	.	.	PUNCT
eurjchem-1783	84	3	calcd	calcd	NOUN
eurjchem-1783	84	4	.	.	PUNCT
eurjchem-1783	85	1	for	for	SCONJ
eurjchem-1783	85	2	c10h13fn2o	c10h13fn2o	PROPN
eurjchem-1783	85	3	:	:	PUNCT
eurjchem-1783	85	4	c	c	X
eurjchem-1783	85	5	,	,	PUNCT
eurjchem-1783	85	6	61.21	61.21	NUM
eurjchem-1783	85	7	;	;	PUNCT
eurjchem-1783	85	8	h	h	X
eurjchem-1783	85	9	,	,	PUNCT
eurjchem-1783	85	10	6.68	6.68	NUM
eurjchem-1783	85	11	;	;	PUNCT
eurjchem-1783	85	12	n	n	CCONJ
eurjchem-1783	85	13	,	,	PUNCT
eurjchem-1783	85	14	14.28	14.28	NUM
eurjchem-1783	85	15	.	.	PUNCT
eurjchem-1783	85	16	found	find	VERB
eurjchem-1783	85	17	:	:	PUNCT
eurjchem-1783	86	1	c	c	X
eurjchem-1783	86	2	,	,	PUNCT
eurjchem-1783	86	3	61.11	61.11	NUM
eurjchem-1783	86	4	;	;	PUNCT
eurjchem-1783	86	5	h	h	NOUN
eurjchem-1783	86	6	,	,	PUNCT
eurjchem-1783	86	7	6.48	6.48	NUM
eurjchem-1783	86	8	;	;	PUNCT
eurjchem-1783	86	9	n	n	CCONJ
eurjchem-1783	86	10	,	,	PUNCT
eurjchem-1783	86	11	14.12	14.12	NUM
eurjchem-1783	86	12	%	%	NOUN
eurjchem-1783	86	13	.	.	PUNCT
eurjchem-1783	87	1	2018	2018	NUM
eurjchem-1783	87	2	–	–	PUNCT
eurjchem-1783	87	3	european	european	ADJ
eurjchem-1783	87	4	journal	journal	NOUN
eurjchem-1783	87	5	of	of	ADP
eurjchem-1783	87	6	chemistry	chemistry	NOUN
eurjchem-1783	87	7	–	–	PUNCT
eurjchem-1783	87	8	cc	cc	NOUN
eurjchem-1783	87	9	by	by	ADP
eurjchem-1783	87	10	nc	nc	PROPN
eurjchem-1783	87	11	–	–	PUNCT
eurjchem-1783	87	12	doi	doi	PROPN
eurjchem-1783	87	13	:	:	PUNCT
eurjchem-1783	87	14	10.5155	10.5155	NUM
eurjchem-1783	87	15	/	/	SYM
eurjchem-1783	87	16	eurjchem.9.4.353	eurjchem.9.4.353	PROPN
eurjchem-1783	87	17	-	-	SYM
eurjchem-1783	87	18	359.1783	359.1783	NUM
eurjchem-1783	87	19	siddaraj	siddaraj	ADJ
eurjchem-1783	87	20	et	et	NOUN
eurjchem-1783	87	21	al	al	PROPN
eurjchem-1783	87	22	.	.	PUNCT
eurjchem-1783	87	23	/	/	SYM
eurjchem-1783	87	24	european	european	PROPN
eurjchem-1783	87	25	journal	journal	PROPN
eurjchem-1783	87	26	of	of	ADP
eurjchem-1783	87	27	chemistry	chemistry	NOUN
eurjchem-1783	87	28	9	9	NUM
eurjchem-1783	87	29	(	(	PUNCT
eurjchem-1783	87	30	4	4	NUM
eurjchem-1783	87	31	)	)	PUNCT
eurjchem-1783	87	32	(	(	PUNCT
eurjchem-1783	87	33	2018	2018	NUM
eurjchem-1783	87	34	)	)	PUNCT
eurjchem-1783	88	1	353	353	NUM
eurjchem-1783	88	2	-	-	SYM
eurjchem-1783	88	3	359	359	NUM
eurjchem-1783	88	4	355	355	NUM
eurjchem-1783	88	5	n	n	NUM
eurjchem-1783	88	6	h	h	NOUN
eurjchem-1783	89	1	o	o	NOUN
eurjchem-1783	89	2	f	f	PROPN
eurjchem-1783	89	3	f	f	PROPN
eurjchem-1783	89	4	no2	no2	PROPN
eurjchem-1783	89	5	n	n	CCONJ
eurjchem-1783	89	6	f	f	PROPN
eurjchem-1783	89	7	no2	no2	NOUN
eurjchem-1783	89	8	o	o	NOUN
eurjchem-1783	90	1	n	n	CCONJ
eurjchem-1783	90	2	f	f	PROPN
eurjchem-1783	90	3	nh2	nh2	PROPN
eurjchem-1783	90	4	o	o	PROPN
eurjchem-1783	91	1	n	n	CCONJ
eurjchem-1783	91	2	f	f	NOUN
eurjchem-1783	92	1	hn	hn	NOUN
eurjchem-1783	93	1	o	o	X
eurjchem-1783	93	2	o	o	X
eurjchem-1783	93	3	o	o	X
eurjchem-1783	94	1	n	n	CCONJ
eurjchem-1783	94	2	f	f	PROPN
eurjchem-1783	94	3	n	n	PRON
eurjchem-1783	95	1	o	o	NOUN
eurjchem-1783	95	2	o	o	X
eurjchem-1783	95	3	o	o	X
eurjchem-1783	95	4	br	br	INTJ
eurjchem-1783	96	1	n	n	NOUN
eurjchem-1783	96	2	f	f	PROPN
eurjchem-1783	96	3	n	n	ADV
eurjchem-1783	96	4	o	o	NOUN
eurjchem-1783	96	5	o	o	X
eurjchem-1783	96	6	o	o	X
eurjchem-1783	96	7	h	h	NOUN
eurjchem-1783	97	1	n	n	ADV
eurjchem-1783	97	2	o	o	NOUN
eurjchem-1783	98	1	a	a	DET
eurjchem-1783	98	2	b	b	X
eurjchem-1783	98	3	c	c	X
eurjchem-1783	98	4	de	de	X
eurjchem-1783	98	5	1	1	NUM
eurjchem-1783	98	6	2	2	NUM
eurjchem-1783	98	7	345	345	NUM
eurjchem-1783	98	8	reagents	reagent	NOUN
eurjchem-1783	98	9	and	and	CCONJ
eurjchem-1783	98	10	conditions	condition	NOUN
eurjchem-1783	98	11	:	:	PUNCT
eurjchem-1783	98	12	a	a	X
eurjchem-1783	98	13	)	)	PUNCT
eurjchem-1783	98	14	tea	tea	NOUN
eurjchem-1783	98	15	,	,	PUNCT
eurjchem-1783	98	16	thf	thf	NOUN
eurjchem-1783	98	17	;	;	PUNCT
eurjchem-1783	98	18	b	b	X
eurjchem-1783	98	19	)	)	PUNCT
eurjchem-1783	98	20	raney	raney	PROPN
eurjchem-1783	98	21	ni	ni	PROPN
eurjchem-1783	98	22	,	,	PUNCT
eurjchem-1783	98	23	nh2nh2	nh2nh2	NOUN
eurjchem-1783	98	24	,	,	PUNCT
eurjchem-1783	98	25	etoh	etoh	NOUN
eurjchem-1783	98	26	;	;	PUNCT
eurjchem-1783	98	27	c	c	X
eurjchem-1783	98	28	)	)	PUNCT
eurjchem-1783	98	29	cbz	cbz	NOUN
eurjchem-1783	98	30	-	-	PUNCT
eurjchem-1783	98	31	cl	cl	NOUN
eurjchem-1783	98	32	,	,	PUNCT
eurjchem-1783	98	33	thf	thf	NOUN
eurjchem-1783	98	34	;	;	PUNCT
eurjchem-1783	98	35	d	d	X
eurjchem-1783	98	36	)	)	PUNCT
eurjchem-1783	98	37	2-(bromomethyl)oxirane	2-(bromomethyl)oxirane	NUM
eurjchem-1783	98	38	,	,	PUNCT
eurjchem-1783	98	39	csco3	csco3	ADJ
eurjchem-1783	98	40	,	,	PUNCT
eurjchem-1783	98	41	ch3cn	ch3cn	NUM
eurjchem-1783	98	42	;	;	PUNCT
eurjchem-1783	98	43	e	e	X
eurjchem-1783	98	44	)	)	PUNCT
eurjchem-1783	98	45	acetamide	acetamide	NOUN
eurjchem-1783	98	46	,	,	PUNCT
eurjchem-1783	98	47	csco3	csco3	PROPN
eurjchem-1783	98	48	,	,	PUNCT
eurjchem-1783	98	49	nai	nai	PROPN
eurjchem-1783	98	50	,	,	PUNCT
eurjchem-1783	98	51	ch3cn	ch3cn	NUM
eurjchem-1783	98	52	.	.	PUNCT
eurjchem-1783	98	53	scheme	scheme	NOUN
eurjchem-1783	98	54	2	2	NUM
eurjchem-1783	98	55	2.2.3	2.2.3	NUM
eurjchem-1783	98	56	.	.	PUNCT
eurjchem-1783	99	1	synthesis	synthesis	NOUN
eurjchem-1783	99	2	of	of	ADP
eurjchem-1783	99	3	benzyl	benzyl	NOUN
eurjchem-1783	99	4	(	(	PUNCT
eurjchem-1783	99	5	3	3	NUM
eurjchem-1783	99	6	-	-	PUNCT
eurjchem-1783	99	7	fluoro-4	fluoro-4	NOUN
eurjchem-1783	99	8	-	-	PUNCT
eurjchem-1783	99	9	morpholinophenyl	morpholinophenyl	NOUN
eurjchem-1783	99	10	)	)	PUNCT
eurjchem-1783	99	11	carbamate	carbamate	NOUN
eurjchem-1783	99	12	(	(	PUNCT
eurjchem-1783	99	13	3	3	NUM
eurjchem-1783	99	14	)	)	PUNCT
eurjchem-1783	99	15	3	3	NUM
eurjchem-1783	99	16	-	-	PUNCT
eurjchem-1783	99	17	fluoro-4	fluoro-4	NOUN
eurjchem-1783	99	18	-	-	PUNCT
eurjchem-1783	99	19	morpholinoaniline	morpholinoaniline	NOUN
eurjchem-1783	99	20	(	(	PUNCT
eurjchem-1783	99	21	22	22	NUM
eurjchem-1783	99	22	g	g	NOUN
eurjchem-1783	99	23	,	,	PUNCT
eurjchem-1783	99	24	0.112	0.112	NUM
eurjchem-1783	99	25	mol	mol	NOUN
eurjchem-1783	99	26	)	)	PUNCT
eurjchem-1783	99	27	was	be	AUX
eurjchem-1783	99	28	dissolved	dissolve	VERB
eurjchem-1783	99	29	in	in	ADP
eurjchem-1783	99	30	dry	dry	ADJ
eurjchem-1783	99	31	thf	thf	NOUN
eurjchem-1783	99	32	(	(	PUNCT
eurjchem-1783	99	33	170	170	NUM
eurjchem-1783	99	34	ml	ml	NOUN
eurjchem-1783	99	35	)	)	PUNCT
eurjchem-1783	99	36	.	.	PUNCT
eurjchem-1783	100	1	added	add	VERB
eurjchem-1783	100	2	triethyl	triethyl	PROPN
eurjchem-1783	100	3	amine	amine	PROPN
eurjchem-1783	100	4	(	(	PUNCT
eurjchem-1783	100	5	12.47	12.47	NUM
eurjchem-1783	100	6	g	g	NOUN
eurjchem-1783	100	7	,	,	PUNCT
eurjchem-1783	100	8	0.123	0.123	NUM
eurjchem-1783	100	9	mol	mol	NOUN
eurjchem-1783	100	10	)	)	PUNCT
eurjchem-1783	100	11	and	and	CCONJ
eurjchem-1783	100	12	cooled	cool	VERB
eurjchem-1783	100	13	to	to	ADP
eurjchem-1783	100	14	-10	-10	PUNCT
eurjchem-1783	100	15	°	°	PRON
eurjchem-1783	100	16	c	c	NOUN
eurjchem-1783	100	17	.	.	PUNCT
eurjchem-1783	100	18	benzyl	benzyl	NOUN
eurjchem-1783	100	19	chloroformate	chloroformate	NOUN
eurjchem-1783	100	20	(	(	PUNCT
eurjchem-1783	100	21	20.03	20.03	NUM
eurjchem-1783	100	22	g	g	NOUN
eurjchem-1783	100	23	,	,	PUNCT
eurjchem-1783	100	24	0.117	0.117	NUM
eurjchem-1783	100	25	mol	mol	NOUN
eurjchem-1783	100	26	)	)	PUNCT
eurjchem-1783	100	27	diluted	dilute	VERB
eurjchem-1783	100	28	with	with	ADP
eurjchem-1783	100	29	thf	thf	NOUN
eurjchem-1783	100	30	(	(	PUNCT
eurjchem-1783	100	31	50	50	NUM
eurjchem-1783	100	32	ml	ml	NOUN
eurjchem-1783	100	33	)	)	PUNCT
eurjchem-1783	100	34	was	be	AUX
eurjchem-1783	100	35	slowly	slowly	ADV
eurjchem-1783	100	36	added	add	VERB
eurjchem-1783	100	37	in	in	ADP
eurjchem-1783	100	38	to	to	ADP
eurjchem-1783	100	39	the	the	DET
eurjchem-1783	100	40	flask	flask	NOUN
eurjchem-1783	100	41	by	by	ADP
eurjchem-1783	100	42	keeping	keep	VERB
eurjchem-1783	100	43	the	the	DET
eurjchem-1783	100	44	temperature	temperature	NOUN
eurjchem-1783	100	45	below	below	ADP
eurjchem-1783	100	46	0	0	NUM
eurjchem-1783	101	1	°	°	DET
eurjchem-1783	101	2	c	c	NOUN
eurjchem-1783	101	3	.	.	PUNCT
eurjchem-1783	102	1	after	after	SCONJ
eurjchem-1783	102	2	the	the	DET
eurjchem-1783	102	3	completion	completion	NOUN
eurjchem-1783	102	4	of	of	ADP
eurjchem-1783	102	5	addition	addition	NOUN
eurjchem-1783	102	6	cooling	cool	VERB
eurjchem-1783	102	7	bath	bath	NOUN
eurjchem-1783	102	8	is	be	AUX
eurjchem-1783	102	9	removed	remove	VERB
eurjchem-1783	102	10	and	and	CCONJ
eurjchem-1783	102	11	reaction	reaction	NOUN
eurjchem-1783	102	12	mixture	mixture	NOUN
eurjchem-1783	102	13	was	be	AUX
eurjchem-1783	102	14	warmed	warm	VERB
eurjchem-1783	102	15	to	to	ADP
eurjchem-1783	102	16	room	room	NOUN
eurjchem-1783	102	17	temperature	temperature	NOUN
eurjchem-1783	102	18	and	and	CCONJ
eurjchem-1783	102	19	stirred	stir	VERB
eurjchem-1783	102	20	at	at	ADP
eurjchem-1783	102	21	the	the	DET
eurjchem-1783	102	22	same	same	ADJ
eurjchem-1783	102	23	for	for	ADP
eurjchem-1783	102	24	1	1	NUM
eurjchem-1783	102	25	hr	hr	NOUN
eurjchem-1783	102	26	.	.	PUNCT
eurjchem-1783	103	1	completion	completion	NOUN
eurjchem-1783	103	2	of	of	ADP
eurjchem-1783	103	3	the	the	DET
eurjchem-1783	103	4	reaction	reaction	NOUN
eurjchem-1783	103	5	is	be	AUX
eurjchem-1783	103	6	monitored	monitor	VERB
eurjchem-1783	103	7	by	by	ADP
eurjchem-1783	103	8	tlc	tlc	PROPN
eurjchem-1783	103	9	.	.	PUNCT
eurjchem-1783	104	1	ethyl	ethyl	PROPN
eurjchem-1783	104	2	acetate	acetate	PROPN
eurjchem-1783	104	3	(	(	PUNCT
eurjchem-1783	104	4	150	150	NUM
eurjchem-1783	104	5	ml	ml	NOUN
eurjchem-1783	104	6	)	)	PUNCT
eurjchem-1783	104	7	and	and	CCONJ
eurjchem-1783	104	8	water	water	NOUN
eurjchem-1783	104	9	(	(	PUNCT
eurjchem-1783	104	10	100	100	NUM
eurjchem-1783	104	11	ml	ml	NOUN
eurjchem-1783	104	12	)	)	PUNCT
eurjchem-1783	104	13	were	be	AUX
eurjchem-1783	104	14	added	add	VERB
eurjchem-1783	104	15	,	,	PUNCT
eurjchem-1783	104	16	organic	organic	ADJ
eurjchem-1783	104	17	layer	layer	NOUN
eurjchem-1783	104	18	was	be	AUX
eurjchem-1783	104	19	separated	separate	VERB
eurjchem-1783	104	20	,	,	PUNCT
eurjchem-1783	104	21	and	and	CCONJ
eurjchem-1783	104	22	aqueous	aqueous	ADJ
eurjchem-1783	104	23	layer	layer	NOUN
eurjchem-1783	104	24	was	be	AUX
eurjchem-1783	104	25	extracted	extract	VERB
eurjchem-1783	104	26	with	with	ADP
eurjchem-1783	104	27	ethyl	ethyl	PROPN
eurjchem-1783	104	28	acetate	acetate	NOUN
eurjchem-1783	104	29	(	(	PUNCT
eurjchem-1783	104	30	2×75	2×75	NUM
eurjchem-1783	104	31	ml	ml	NOUN
eurjchem-1783	104	32	)	)	PUNCT
eurjchem-1783	104	33	,	,	PUNCT
eurjchem-1783	104	34	combined	combine	VERB
eurjchem-1783	104	35	organic	organic	ADJ
eurjchem-1783	104	36	layer	layer	NOUN
eurjchem-1783	104	37	was	be	AUX
eurjchem-1783	104	38	washed	wash	VERB
eurjchem-1783	104	39	with	with	ADP
eurjchem-1783	104	40	water	water	NOUN
eurjchem-1783	104	41	(	(	PUNCT
eurjchem-1783	104	42	2×70	2×70	NUM
eurjchem-1783	104	43	ml	ml	NOUN
eurjchem-1783	104	44	)	)	PUNCT
eurjchem-1783	104	45	,	,	PUNCT
eurjchem-1783	104	46	brine	brine	NOUN
eurjchem-1783	104	47	(	(	PUNCT
eurjchem-1783	104	48	75	75	NUM
eurjchem-1783	104	49	ml	ml	NOUN
eurjchem-1783	104	50	)	)	PUNCT
eurjchem-1783	104	51	,	,	PUNCT
eurjchem-1783	104	52	dried	dry	VERB
eurjchem-1783	104	53	over	over	ADP
eurjchem-1783	104	54	na2so4	na2so4	NOUN
eurjchem-1783	104	55	,	,	PUNCT
eurjchem-1783	104	56	filtered	filter	VERB
eurjchem-1783	104	57	and	and	CCONJ
eurjchem-1783	104	58	concentrated	concentrate	VERB
eurjchem-1783	104	59	to	to	PART
eurjchem-1783	104	60	obtain	obtain	VERB
eurjchem-1783	104	61	the	the	DET
eurjchem-1783	104	62	crude	crude	ADJ
eurjchem-1783	104	63	product	product	NOUN
eurjchem-1783	104	64	.	.	PUNCT
eurjchem-1783	105	1	crude	crude	ADJ
eurjchem-1783	105	2	product	product	NOUN
eurjchem-1783	105	3	obtained	obtain	VERB
eurjchem-1783	105	4	was	be	AUX
eurjchem-1783	105	5	added	add	VERB
eurjchem-1783	105	6	hexane	hexane	NOUN
eurjchem-1783	105	7	:	:	PUNCT
eurjchem-1783	105	8	diethyl	diethyl	NOUN
eurjchem-1783	105	9	ether	ether	NOUN
eurjchem-1783	105	10	(	(	PUNCT
eurjchem-1783	105	11	9:1	9:1	NUM
eurjchem-1783	105	12	,	,	PUNCT
eurjchem-1783	105	13	v	v	NOUN
eurjchem-1783	105	14	:	:	PUNCT
eurjchem-1783	105	15	v	v	NOUN
eurjchem-1783	105	16	)	)	PUNCT
eurjchem-1783	105	17	for	for	ADP
eurjchem-1783	105	18	10	10	NUM
eurjchem-1783	105	19	mins	min	NOUN
eurjchem-1783	105	20	.	.	PUNCT
eurjchem-1783	106	1	filtered	filter	VERB
eurjchem-1783	106	2	and	and	CCONJ
eurjchem-1783	106	3	dried	dry	VERB
eurjchem-1783	106	4	to	to	PART
eurjchem-1783	106	5	get	get	VERB
eurjchem-1783	106	6	a	a	DET
eurjchem-1783	106	7	pure	pure	ADJ
eurjchem-1783	106	8	product	product	NOUN
eurjchem-1783	106	9	as	as	ADP
eurjchem-1783	106	10	off	off	ADP
eurjchem-1783	106	11	white	white	ADJ
eurjchem-1783	106	12	solid	solid	ADJ
eurjchem-1783	106	13	(	(	PUNCT
eurjchem-1783	106	14	scheme	scheme	NOUN
eurjchem-1783	106	15	2	2	NUM
eurjchem-1783	106	16	)	)	PUNCT
eurjchem-1783	106	17	.	.	PUNCT
eurjchem-1783	107	1	color	color	NOUN
eurjchem-1783	107	2	:	:	PUNCT
eurjchem-1783	107	3	off	off	ADP
eurjchem-1783	107	4	white	white	PROPN
eurjchem-1783	107	5	.	.	PUNCT
eurjchem-1783	108	1	yield	yield	NOUN
eurjchem-1783	108	2	:	:	PUNCT
eurjchem-1783	108	3	87	87	NUM
eurjchem-1783	108	4	%	%	NOUN
eurjchem-1783	108	5	.	.	PUNCT
eurjchem-1783	109	1	m.p	m.p	PROPN
eurjchem-1783	109	2	.	.	PROPN
eurjchem-1783	109	3	:	:	PUNCT
eurjchem-1783	110	1	126127	126127	NUM
eurjchem-1783	110	2	°	°	SYM
eurjchem-1783	110	3	c	c	X
eurjchem-1783	110	4	.	.	PUNCT
eurjchem-1783	111	1	1h	1h	NUM
eurjchem-1783	111	2	nmr	nmr	NOUN
eurjchem-1783	111	3	(	(	PUNCT
eurjchem-1783	111	4	400	400	NUM
eurjchem-1783	111	5	mhz	mhz	NOUN
eurjchem-1783	111	6	,	,	PUNCT
eurjchem-1783	111	7	cdcl3	cdcl3	PROPN
eurjchem-1783	111	8	,	,	PUNCT
eurjchem-1783	111	9	δ	δ	PROPN
eurjchem-1783	111	10	,	,	PUNCT
eurjchem-1783	111	11	ppm	ppm	NOUN
eurjchem-1783	111	12	):	):	PUNCT
eurjchem-1783	111	13	7.27	7.27	NUM
eurjchem-1783	111	14	-	-	SYM
eurjchem-1783	111	15	7.33	7.33	NUM
eurjchem-1783	111	16	(	(	PUNCT
eurjchem-1783	111	17	m	m	PROPN
eurjchem-1783	111	18	,	,	PUNCT
eurjchem-1783	111	19	5h	5h	NUM
eurjchem-1783	111	20	,	,	PUNCT
eurjchem-1783	111	21	ar	ar	NOUN
eurjchem-1783	111	22	-	-	NOUN
eurjchem-1783	111	23	h	h	NOUN
eurjchem-1783	111	24	)	)	PUNCT
eurjchem-1783	111	25	,	,	PUNCT
eurjchem-1783	111	26	7.08	7.08	NUM
eurjchem-1783	111	27	(	(	PUNCT
eurjchem-1783	111	28	dd	dd	PROPN
eurjchem-1783	111	29	,	,	PUNCT
eurjchem-1783	111	30	j	j	NOUN
eurjchem-1783	111	31	=	=	SYM
eurjchem-1783	111	32	4	4	NUM
eurjchem-1783	111	33	hz	hz	NOUN
eurjchem-1783	111	34	,	,	PUNCT
eurjchem-1783	111	35	1h	1h	NUM
eurjchem-1783	111	36	,	,	PUNCT
eurjchem-1783	111	37	ar	ar	NOUN
eurjchem-1783	111	38	-	-	NOUN
eurjchem-1783	111	39	h	h	NOUN
eurjchem-1783	111	40	)	)	PUNCT
eurjchem-1783	111	41	6.93	6.93	NUM
eurjchem-1783	111	42	(	(	PUNCT
eurjchem-1783	111	43	d	d	NOUN
eurjchem-1783	111	44	,	,	PUNCT
eurjchem-1783	111	45	j	j	PROPN
eurjchem-1783	111	46	=	=	SYM
eurjchem-1783	111	47	4	4	NUM
eurjchem-1783	111	48	hz	hz	NOUN
eurjchem-1783	111	49	,	,	PUNCT
eurjchem-1783	111	50	2h	2h	NUM
eurjchem-1783	111	51	,	,	PUNCT
eurjchem-1783	111	52	ar	ar	NOUN
eurjchem-1783	111	53	-	-	NOUN
eurjchem-1783	111	54	h	h	NOUN
eurjchem-1783	111	55	)	)	PUNCT
eurjchem-1783	111	56	,	,	PUNCT
eurjchem-1783	111	57	5.10	5.10	NUM
eurjchem-1783	111	58	(	(	PUNCT
eurjchem-1783	111	59	s	s	PROPN
eurjchem-1783	111	60	,	,	PUNCT
eurjchem-1783	111	61	2h	2h	NUM
eurjchem-1783	111	62	,	,	PUNCT
eurjchem-1783	111	63	ar	ar	NOUN
eurjchem-1783	111	64	-	-	NOUN
eurjchem-1783	111	65	ch2	ch2	NOUN
eurjchem-1783	111	66	)	)	PUNCT
eurjchem-1783	111	67	,	,	PUNCT
eurjchem-1783	111	68	3.83	3.83	NUM
eurjchem-1783	111	69	(	(	PUNCT
eurjchem-1783	111	70	t	t	PROPN
eurjchem-1783	111	71	,	,	PUNCT
eurjchem-1783	111	72	j	j	PROPN
eurjchem-1783	112	1	=	=	SYM
eurjchem-1783	112	2	2.1	2.1	NUM
eurjchem-1783	112	3	hz	hz	NOUN
eurjchem-1783	112	4	,	,	PUNCT
eurjchem-1783	112	5	4h	4h	NOUN
eurjchem-1783	112	6	,	,	PUNCT
eurjchem-1783	112	7	morpholine	morpholine	NOUN
eurjchem-1783	112	8	-	-	PUNCT
eurjchem-1783	112	9	ch2	ch2	NOUN
eurjchem-1783	112	10	)	)	PUNCT
eurjchem-1783	112	11	,	,	PUNCT
eurjchem-1783	112	12	3.00	3.00	NUM
eurjchem-1783	112	13	(	(	PUNCT
eurjchem-1783	112	14	t	t	PROPN
eurjchem-1783	112	15	,	,	PUNCT
eurjchem-1783	112	16	j	j	PROPN
eurjchem-1783	112	17	=	=	SYM
eurjchem-1783	112	18	2.1	2.1	NUM
eurjchem-1783	112	19	hz	hz	NOUN
eurjchem-1783	112	20	,	,	PUNCT
eurjchem-1783	112	21	4h	4h	NOUN
eurjchem-1783	112	22	,	,	PUNCT
eurjchem-1783	112	23	morpholine	morpholine	NOUN
eurjchem-1783	112	24	-	-	PUNCT
eurjchem-1783	112	25	ch2	ch2	NOUN
eurjchem-1783	112	26	)	)	PUNCT
eurjchem-1783	112	27	.	.	PUNCT
eurjchem-1783	113	1	13c	13c	NOUN
eurjchem-1783	113	2	nmr	nmr	NOUN
eurjchem-1783	113	3	(	(	PUNCT
eurjchem-1783	113	4	100	100	NUM
eurjchem-1783	113	5	mhz	mhz	NOUN
eurjchem-1783	113	6	,	,	PUNCT
eurjchem-1783	113	7	cdcl3	cdcl3	PROPN
eurjchem-1783	113	8	,	,	PUNCT
eurjchem-1783	113	9	δ	δ	PROPN
eurjchem-1783	113	10	,	,	PUNCT
eurjchem-1783	113	11	ppm	ppm	NUM
eurjchem-1783	113	12	):	):	PUNCT
eurjchem-1783	113	13	156.1	156.1	NUM
eurjchem-1783	113	14	(	(	PUNCT
eurjchem-1783	113	15	1c	1c	NOUN
eurjchem-1783	113	16	,	,	PUNCT
eurjchem-1783	113	17	co	co	NOUN
eurjchem-1783	113	18	)	)	PUNCT
eurjchem-1783	113	19	,	,	PUNCT
eurjchem-1783	113	20	147.4	147.4	NUM
eurjchem-1783	113	21	(	(	PUNCT
eurjchem-1783	113	22	1c	1c	NOUN
eurjchem-1783	113	23	,	,	PUNCT
eurjchem-1783	113	24	ar	ar	NOUN
eurjchem-1783	113	25	-	-	NOUN
eurjchem-1783	113	26	c	c	NOUN
eurjchem-1783	113	27	)	)	PUNCT
eurjchem-1783	113	28	,	,	PUNCT
eurjchem-1783	113	29	137.3	137.3	NUM
eurjchem-1783	113	30	(	(	PUNCT
eurjchem-1783	113	31	1c	1c	NOUN
eurjchem-1783	113	32	,	,	PUNCT
eurjchem-1783	113	33	arc	arc	NOUN
eurjchem-1783	113	34	)	)	PUNCT
eurjchem-1783	113	35	,	,	PUNCT
eurjchem-1783	113	36	136.1	136.1	NUM
eurjchem-1783	113	37	(	(	PUNCT
eurjchem-1783	113	38	1c	1c	NOUN
eurjchem-1783	113	39	,	,	PUNCT
eurjchem-1783	113	40	ar	ar	NOUN
eurjchem-1783	113	41	-	-	NOUN
eurjchem-1783	113	42	c	c	NOUN
eurjchem-1783	113	43	)	)	PUNCT
eurjchem-1783	113	44	,	,	PUNCT
eurjchem-1783	113	45	129.6	129.6	NUM
eurjchem-1783	113	46	(	(	PUNCT
eurjchem-1783	113	47	1c	1c	NOUN
eurjchem-1783	113	48	,	,	PUNCT
eurjchem-1783	113	49	ar	ar	NOUN
eurjchem-1783	113	50	-	-	NOUN
eurjchem-1783	113	51	c	c	NOUN
eurjchem-1783	113	52	)	)	PUNCT
eurjchem-1783	113	53	,	,	PUNCT
eurjchem-1783	113	54	128.4	128.4	NUM
eurjchem-1783	113	55	(	(	PUNCT
eurjchem-1783	113	56	2c	2c	NUM
eurjchem-1783	113	57	,	,	PUNCT
eurjchem-1783	113	58	ar	ar	NOUN
eurjchem-1783	113	59	-	-	NOUN
eurjchem-1783	113	60	c	c	NOUN
eurjchem-1783	113	61	)	)	PUNCT
eurjchem-1783	113	62	,	,	PUNCT
eurjchem-1783	113	63	127.9	127.9	NUM
eurjchem-1783	113	64	(	(	PUNCT
eurjchem-1783	113	65	2c	2c	NUM
eurjchem-1783	113	66	,	,	PUNCT
eurjchem-1783	113	67	ar	ar	NOUN
eurjchem-1783	113	68	-	-	NOUN
eurjchem-1783	113	69	c	c	NOUN
eurjchem-1783	113	70	)	)	PUNCT
eurjchem-1783	113	71	,	,	PUNCT
eurjchem-1783	113	72	127.5	127.5	NUM
eurjchem-1783	113	73	(	(	PUNCT
eurjchem-1783	113	74	2c	2c	NUM
eurjchem-1783	113	75	,	,	PUNCT
eurjchem-1783	113	76	ar	ar	NOUN
eurjchem-1783	113	77	-	-	NOUN
eurjchem-1783	113	78	c	c	NOUN
eurjchem-1783	113	79	)	)	PUNCT
eurjchem-1783	113	80	,	,	PUNCT
eurjchem-1783	113	81	126.3	126.3	NUM
eurjchem-1783	113	82	(	(	PUNCT
eurjchem-1783	113	83	1c	1c	NOUN
eurjchem-1783	113	84	,	,	PUNCT
eurjchem-1783	113	85	ar	ar	NOUN
eurjchem-1783	113	86	-	-	NOUN
eurjchem-1783	113	87	c	c	NOUN
eurjchem-1783	113	88	)	)	PUNCT
eurjchem-1783	113	89	,	,	PUNCT
eurjchem-1783	113	90	120.21	120.21	NUM
eurjchem-1783	113	91	(	(	PUNCT
eurjchem-1783	113	92	1c	1c	NUM
eurjchem-1783	113	93	,	,	PUNCT
eurjchem-1783	113	94	arc	arc	NOUN
eurjchem-1783	113	95	)	)	PUNCT
eurjchem-1783	113	96	,	,	PUNCT
eurjchem-1783	113	97	67.46	67.46	NUM
eurjchem-1783	113	98	(	(	PUNCT
eurjchem-1783	113	99	1c	1c	NOUN
eurjchem-1783	113	100	,	,	PUNCT
eurjchem-1783	113	101	ch2	ch2	PROPN
eurjchem-1783	113	102	)	)	PUNCT
eurjchem-1783	113	103	,	,	PUNCT
eurjchem-1783	113	104	66.9	66.9	NUM
eurjchem-1783	113	105	(	(	PUNCT
eurjchem-1783	113	106	2c	2c	NUM
eurjchem-1783	113	107	,	,	PUNCT
eurjchem-1783	113	108	morpholine	morpholine	NOUN
eurjchem-1783	113	109	-	-	PUNCT
eurjchem-1783	113	110	c	c	NOUN
eurjchem-1783	113	111	)	)	PUNCT
eurjchem-1783	113	112	,	,	PUNCT
eurjchem-1783	113	113	51.47	51.47	NUM
eurjchem-1783	113	114	(	(	PUNCT
eurjchem-1783	113	115	2c	2c	NUM
eurjchem-1783	113	116	,	,	PUNCT
eurjchem-1783	113	117	morpholine	morpholine	NOUN
eurjchem-1783	113	118	-	-	PUNCT
eurjchem-1783	113	119	c	c	NOUN
eurjchem-1783	113	120	)	)	PUNCT
eurjchem-1783	113	121	.	.	PUNCT
eurjchem-1783	114	1	ms	ms	NOUN
eurjchem-1783	114	2	(	(	PUNCT
eurjchem-1783	114	3	m	m	PROPN
eurjchem-1783	114	4	/	/	SYM
eurjchem-1783	114	5	z	z	PROPN
eurjchem-1783	114	6	):	):	PUNCT
eurjchem-1783	114	7	331.3	331.3	NUM
eurjchem-1783	114	8	(	(	PUNCT
eurjchem-1783	114	9	m+	m+	NUM
eurjchem-1783	114	10	)	)	PUNCT
eurjchem-1783	114	11	.	.	PUNCT
eurjchem-1783	115	1	anal	anal	PROPN
eurjchem-1783	115	2	.	.	PUNCT
eurjchem-1783	115	3	calcd	calcd	NOUN
eurjchem-1783	115	4	.	.	PUNCT
eurjchem-1783	116	1	for	for	ADP
eurjchem-1783	116	2	c18h19fn2o3	c18h19fn2o3	NOUN
eurjchem-1783	116	3	:	:	PUNCT
eurjchem-1783	116	4	c	c	X
eurjchem-1783	116	5	,	,	PUNCT
eurjchem-1783	116	6	65.44	65.44	NUM
eurjchem-1783	116	7	;	;	PUNCT
eurjchem-1783	116	8	h	h	NOUN
eurjchem-1783	116	9	,	,	PUNCT
eurjchem-1783	116	10	5.80	5.80	NUM
eurjchem-1783	116	11	;	;	PUNCT
eurjchem-1783	116	12	n	n	CCONJ
eurjchem-1783	116	13	,	,	PUNCT
eurjchem-1783	116	14	8.48	8.48	NUM
eurjchem-1783	116	15	.	.	PUNCT
eurjchem-1783	116	16	found	find	VERB
eurjchem-1783	116	17	:	:	PUNCT
eurjchem-1783	117	1	c	c	X
eurjchem-1783	117	2	,	,	PUNCT
eurjchem-1783	117	3	65.24	65.24	NUM
eurjchem-1783	117	4	;	;	PUNCT
eurjchem-1783	117	5	h	h	X
eurjchem-1783	117	6	,	,	PUNCT
eurjchem-1783	117	7	5.25	5.25	NUM
eurjchem-1783	117	8	;	;	PUNCT
eurjchem-1783	117	9	n	n	CCONJ
eurjchem-1783	117	10	,	,	PUNCT
eurjchem-1783	117	11	8.51	8.51	NUM
eurjchem-1783	117	12	%	%	NOUN
eurjchem-1783	117	13	.	.	PUNCT
eurjchem-1783	118	1	2.2.4	2.2.4	X
eurjchem-1783	118	2	.	.	X
eurjchem-1783	118	3	synthesis	synthesis	NOUN
eurjchem-1783	118	4	of	of	ADP
eurjchem-1783	118	5	(	(	PUNCT
eurjchem-1783	118	6	r)-5-(bromomethyl)-3-(3	r)-5-(bromomethyl)-3-(3	NOUN
eurjchem-1783	118	7	-	-	PUNCT
eurjchem-1783	118	8	fluoro-4morpholinophenyl	fluoro-4morpholinophenyl	NOUN
eurjchem-1783	118	9	)	)	PUNCT
eurjchem-1783	118	10	oxazolidin-2	oxazolidin-2	NUM
eurjchem-1783	118	11	-	-	SYM
eurjchem-1783	118	12	one	one	NUM
eurjchem-1783	118	13	(	(	PUNCT
eurjchem-1783	118	14	4	4	NUM
eurjchem-1783	118	15	)	)	PUNCT
eurjchem-1783	118	16	benzyl	benzyl	NOUN
eurjchem-1783	118	17	(	(	PUNCT
eurjchem-1783	118	18	3	3	NUM
eurjchem-1783	118	19	-	-	PUNCT
eurjchem-1783	118	20	fluoro-4	fluoro-4	NOUN
eurjchem-1783	118	21	-	-	PUNCT
eurjchem-1783	118	22	morpholinophenyl	morpholinophenyl	NOUN
eurjchem-1783	118	23	)	)	PUNCT
eurjchem-1783	118	24	carbamate	carbamate	NOUN
eurjchem-1783	118	25	(	(	PUNCT
eurjchem-1783	118	26	5	5	NUM
eurjchem-1783	118	27	g	g	NOUN
eurjchem-1783	118	28	,	,	PUNCT
eurjchem-1783	118	29	0.015	0.015	NUM
eurjchem-1783	118	30	mol	mol	NOUN
eurjchem-1783	118	31	)	)	PUNCT
eurjchem-1783	118	32	was	be	AUX
eurjchem-1783	118	33	dissolved	dissolve	VERB
eurjchem-1783	118	34	in	in	ADP
eurjchem-1783	118	35	dry	dry	ADJ
eurjchem-1783	118	36	acetonitrile	acetonitrile	NOUN
eurjchem-1783	118	37	(	(	PUNCT
eurjchem-1783	118	38	100	100	NUM
eurjchem-1783	118	39	ml	ml	NOUN
eurjchem-1783	118	40	)	)	PUNCT
eurjchem-1783	118	41	,	,	PUNCT
eurjchem-1783	118	42	added	add	VERB
eurjchem-1783	118	43	cesium	cesium	NOUN
eurjchem-1783	118	44	carbonate	carbonate	NOUN
eurjchem-1783	118	45	(	(	PUNCT
eurjchem-1783	118	46	5.91	5.91	NUM
eurjchem-1783	118	47	g	g	NOUN
eurjchem-1783	118	48	,	,	PUNCT
eurjchem-1783	118	49	0.018	0.018	NUM
eurjchem-1783	118	50	mol	mol	NOUN
eurjchem-1783	118	51	)	)	PUNCT
eurjchem-1783	118	52	,	,	PUNCT
eurjchem-1783	118	53	(	(	PUNCT
eurjchem-1783	118	54	r)-2-(bromomethyl	r)-2-(bromomethyl	NOUN
eurjchem-1783	118	55	)	)	PUNCT
eurjchem-1783	118	56	oxirane	oxirane	NOUN
eurjchem-1783	118	57	(	(	PUNCT
eurjchem-1783	118	58	2.16	2.16	NUM
eurjchem-1783	118	59	g	g	NOUN
eurjchem-1783	118	60	,	,	PUNCT
eurjchem-1783	118	61	0.016	0.016	NUM
eurjchem-1783	118	62	mol	mol	NOUN
eurjchem-1783	118	63	)	)	PUNCT
eurjchem-1783	118	64	,	,	PUNCT
eurjchem-1783	118	65	stirred	stir	VERB
eurjchem-1783	118	66	at	at	ADP
eurjchem-1783	118	67	room	room	NOUN
eurjchem-1783	118	68	temperature	temperature	NOUN
eurjchem-1783	118	69	for	for	ADP
eurjchem-1783	118	70	10	10	NUM
eurjchem-1783	118	71	min	min	NOUN
eurjchem-1783	118	72	and	and	CCONJ
eurjchem-1783	118	73	refluxed	refluxe	VERB
eurjchem-1783	118	74	for	for	ADP
eurjchem-1783	118	75	4.5	4.5	NUM
eurjchem-1783	118	76	hours	hour	NOUN
eurjchem-1783	118	77	.	.	PUNCT
eurjchem-1783	119	1	reaction	reaction	NOUN
eurjchem-1783	119	2	was	be	AUX
eurjchem-1783	119	3	monitored	monitor	VERB
eurjchem-1783	119	4	by	by	ADP
eurjchem-1783	119	5	tlc	tlc	NOUN
eurjchem-1783	119	6	.	.	PUNCT
eurjchem-1783	120	1	reaction	reaction	NOUN
eurjchem-1783	120	2	mixture	mixture	NOUN
eurjchem-1783	120	3	was	be	AUX
eurjchem-1783	120	4	cooled	cool	VERB
eurjchem-1783	120	5	,	,	PUNCT
eurjchem-1783	120	6	filtered	filter	VERB
eurjchem-1783	120	7	,	,	PUNCT
eurjchem-1783	120	8	concentrated	concentrate	VERB
eurjchem-1783	120	9	to	to	PART
eurjchem-1783	120	10	obtain	obtain	VERB
eurjchem-1783	120	11	crude	crude	ADJ
eurjchem-1783	120	12	compound	compound	NOUN
eurjchem-1783	120	13	which	which	PRON
eurjchem-1783	120	14	was	be	AUX
eurjchem-1783	120	15	further	far	ADV
eurjchem-1783	120	16	purified	purify	VERB
eurjchem-1783	120	17	by	by	ADP
eurjchem-1783	120	18	flash	flash	NOUN
eurjchem-1783	120	19	column	column	NOUN
eurjchem-1783	120	20	chromatography	chromatography	NOUN
eurjchem-1783	120	21	using	use	VERB
eurjchem-1783	120	22	20	20	NUM
eurjchem-1783	120	23	-	-	SYM
eurjchem-1783	120	24	30	30	NUM
eurjchem-1783	120	25	%	%	NOUN
eurjchem-1783	120	26	ethyl	ethyl	PROPN
eurjchem-1783	120	27	acetate	acetate	NOUN
eurjchem-1783	120	28	in	in	ADP
eurjchem-1783	120	29	hexane	hexane	NOUN
eurjchem-1783	120	30	to	to	PART
eurjchem-1783	120	31	obtain	obtain	VERB
eurjchem-1783	120	32	the	the	DET
eurjchem-1783	120	33	product	product	NOUN
eurjchem-1783	120	34	as	as	ADP
eurjchem-1783	120	35	yellow	yellow	ADJ
eurjchem-1783	120	36	color	color	NOUN
eurjchem-1783	120	37	solid	solid	ADJ
eurjchem-1783	120	38	(	(	PUNCT
eurjchem-1783	120	39	scheme	scheme	NOUN
eurjchem-1783	120	40	2	2	NUM
eurjchem-1783	120	41	)	)	PUNCT
eurjchem-1783	120	42	.	.	PUNCT
eurjchem-1783	121	1	color	color	NOUN
eurjchem-1783	121	2	:	:	PUNCT
eurjchem-1783	121	3	yellow	yellow	ADJ
eurjchem-1783	121	4	.	.	PUNCT
eurjchem-1783	122	1	yield	yield	NOUN
eurjchem-1783	122	2	:	:	PUNCT
eurjchem-1783	122	3	96	96	NUM
eurjchem-1783	122	4	%	%	NOUN
eurjchem-1783	122	5	.	.	PUNCT
eurjchem-1783	123	1	m.p	m.p	PROPN
eurjchem-1783	123	2	.	.	PROPN
eurjchem-1783	123	3	:	:	PUNCT
eurjchem-1783	124	1	145	145	NUM
eurjchem-1783	124	2	-	-	SYM
eurjchem-1783	124	3	146	146	NUM
eurjchem-1783	124	4	°	°	PROPN
eurjchem-1783	124	5	c	c	NOUN
eurjchem-1783	124	6	.	.	PUNCT
eurjchem-1783	125	1	1h	1h	NUM
eurjchem-1783	125	2	nmr	nmr	NOUN
eurjchem-1783	125	3	(	(	PUNCT
eurjchem-1783	125	4	400	400	NUM
eurjchem-1783	125	5	mhz	mhz	NOUN
eurjchem-1783	125	6	,	,	PUNCT
eurjchem-1783	125	7	cdcl3	cdcl3	PROPN
eurjchem-1783	125	8	,	,	PUNCT
eurjchem-1783	125	9	δ	δ	PROPN
eurjchem-1783	125	10	,	,	PUNCT
eurjchem-1783	125	11	ppm	ppm	NUM
eurjchem-1783	125	12	):	):	PUNCT
eurjchem-1783	125	13	7.41	7.41	NUM
eurjchem-1783	125	14	(	(	PUNCT
eurjchem-1783	125	15	m	m	PROPN
eurjchem-1783	125	16	,	,	PUNCT
eurjchem-1783	125	17	2h	2h	NUM
eurjchem-1783	125	18	,	,	PUNCT
eurjchem-1783	125	19	ar	ar	NOUN
eurjchem-1783	125	20	-	-	NOUN
eurjchem-1783	125	21	h	h	NOUN
eurjchem-1783	125	22	)	)	PUNCT
eurjchem-1783	125	23	,	,	PUNCT
eurjchem-1783	125	24	6.96	6.96	NUM
eurjchem-1783	125	25	(	(	PUNCT
eurjchem-1783	125	26	m	m	PROPN
eurjchem-1783	125	27	,	,	PUNCT
eurjchem-1783	125	28	1h	1h	NUM
eurjchem-1783	125	29	,	,	PUNCT
eurjchem-1783	125	30	ar	ar	NOUN
eurjchem-1783	125	31	-	-	NOUN
eurjchem-1783	125	32	h	h	NOUN
eurjchem-1783	125	33	)	)	PUNCT
eurjchem-1783	125	34	,	,	PUNCT
eurjchem-1783	125	35	4.71	4.71	NUM
eurjchem-1783	125	36	(	(	PUNCT
eurjchem-1783	125	37	m	m	PROPN
eurjchem-1783	125	38	,	,	PUNCT
eurjchem-1783	125	39	1h	1h	NUM
eurjchem-1783	125	40	,	,	PUNCT
eurjchem-1783	125	41	ch	ch	NOUN
eurjchem-1783	125	42	)	)	PUNCT
eurjchem-1783	125	43	,	,	PUNCT
eurjchem-1783	125	44	4.12	4.12	NUM
eurjchem-1783	125	45	(	(	PUNCT
eurjchem-1783	125	46	t	t	PROPN
eurjchem-1783	125	47	,	,	PUNCT
eurjchem-1783	125	48	j	j	PROPN
eurjchem-1783	125	49	=	=	NOUN
eurjchem-1783	125	50	4	4	NUM
eurjchem-1783	125	51	hz	hz	NOUN
eurjchem-1783	125	52	,	,	PUNCT
eurjchem-1783	125	53	1h	1h	NUM
eurjchem-1783	125	54	,	,	PUNCT
eurjchem-1783	125	55	ch2	ch2	PROPN
eurjchem-1783	125	56	)	)	PUNCT
eurjchem-1783	125	57	3.76	3.76	NUM
eurjchem-1783	125	58	(	(	PUNCT
eurjchem-1783	125	59	t	t	PROPN
eurjchem-1783	125	60	,	,	PUNCT
eurjchem-1783	125	61	j	j	PROPN
eurjchem-1783	126	1	=	=	SYM
eurjchem-1783	126	2	4	4	NUM
eurjchem-1783	126	3	hz	hz	NOUN
eurjchem-1783	126	4	,	,	PUNCT
eurjchem-1783	126	5	4h	4h	NOUN
eurjchem-1783	126	6	,	,	PUNCT
eurjchem-1783	126	7	ch2	ch2	PROPN
eurjchem-1783	126	8	)	)	PUNCT
eurjchem-1783	126	9	,	,	PUNCT
eurjchem-1783	126	10	3.70	3.70	NUM
eurjchem-1783	126	11	(	(	PUNCT
eurjchem-1783	126	12	t	t	PROPN
eurjchem-1783	126	13	,	,	PUNCT
eurjchem-1783	126	14	j	j	PROPN
eurjchem-1783	127	1	=	=	SYM
eurjchem-1783	127	2	4	4	NUM
eurjchem-1783	127	3	hz	hz	NOUN
eurjchem-1783	127	4	,	,	PUNCT
eurjchem-1783	127	5	1h	1h	NUM
eurjchem-1783	127	6	,	,	PUNCT
eurjchem-1783	127	7	ch2	ch2	PROPN
eurjchem-1783	127	8	)	)	PUNCT
eurjchem-1783	127	9	,	,	PUNCT
eurjchem-1783	127	10	3.33	3.33	NUM
eurjchem-1783	127	11	-	-	SYM
eurjchem-1783	127	12	3.43	3.43	NUM
eurjchem-1783	127	13	(	(	PUNCT
eurjchem-1783	127	14	m	m	PROPN
eurjchem-1783	127	15	,	,	PUNCT
eurjchem-1783	127	16	2h	2h	NUM
eurjchem-1783	127	17	,	,	PUNCT
eurjchem-1783	127	18	ch2	ch2	PROPN
eurjchem-1783	127	19	)	)	PUNCT
eurjchem-1783	127	20	,	,	PUNCT
eurjchem-1783	127	21	3.13	3.13	NUM
eurjchem-1783	127	22	(	(	PUNCT
eurjchem-1783	127	23	t	t	PROPN
eurjchem-1783	127	24	,	,	PUNCT
eurjchem-1783	127	25	j	j	PROPN
eurjchem-1783	128	1	=	=	SYM
eurjchem-1783	128	2	4	4	NUM
eurjchem-1783	128	3	hz	hz	NOUN
eurjchem-1783	128	4	,	,	PUNCT
eurjchem-1783	128	5	4h	4h	NOUN
eurjchem-1783	128	6	,	,	PUNCT
eurjchem-1783	128	7	ch2	ch2	PROPN
eurjchem-1783	128	8	)	)	PUNCT
eurjchem-1783	128	9	.	.	PUNCT
eurjchem-1783	129	1	13c	13c	NOUN
eurjchem-1783	129	2	nmr	nmr	NOUN
eurjchem-1783	129	3	(	(	PUNCT
eurjchem-1783	129	4	100	100	NUM
eurjchem-1783	129	5	mhz	mhz	NOUN
eurjchem-1783	129	6	,	,	PUNCT
eurjchem-1783	129	7	cdcl3	cdcl3	PROPN
eurjchem-1783	129	8	,	,	PUNCT
eurjchem-1783	129	9	δ	δ	PROPN
eurjchem-1783	129	10	,	,	PUNCT
eurjchem-1783	129	11	ppm	ppm	NUM
eurjchem-1783	129	12	):	):	PUNCT
eurjchem-1783	129	13	154.9	154.9	NUM
eurjchem-1783	129	14	(	(	PUNCT
eurjchem-1783	129	15	1c	1c	NOUN
eurjchem-1783	129	16	,	,	PUNCT
eurjchem-1783	129	17	co	co	NOUN
eurjchem-1783	129	18	)	)	PUNCT
eurjchem-1783	129	19	,	,	PUNCT
eurjchem-1783	129	20	148.6	148.6	NUM
eurjchem-1783	129	21	(	(	PUNCT
eurjchem-1783	129	22	1c	1c	NOUN
eurjchem-1783	129	23	,	,	PUNCT
eurjchem-1783	129	24	ar	ar	NOUN
eurjchem-1783	129	25	-	-	NOUN
eurjchem-1783	129	26	c	c	NOUN
eurjchem-1783	129	27	)	)	PUNCT
eurjchem-1783	129	28	,	,	PUNCT
eurjchem-1783	129	29	131.26	131.26	NUM
eurjchem-1783	129	30	(	(	PUNCT
eurjchem-1783	129	31	1c	1c	NOUN
eurjchem-1783	129	32	,	,	PUNCT
eurjchem-1783	129	33	ar	ar	NOUN
eurjchem-1783	129	34	-	-	NOUN
eurjchem-1783	129	35	c	c	NOUN
eurjchem-1783	129	36	)	)	PUNCT
eurjchem-1783	129	37	,	,	PUNCT
eurjchem-1783	129	38	129.74	129.74	NUM
eurjchem-1783	129	39	(	(	PUNCT
eurjchem-1783	129	40	1c	1c	NOUN
eurjchem-1783	129	41	,	,	PUNCT
eurjchem-1783	129	42	ar	ar	NOUN
eurjchem-1783	129	43	-	-	NOUN
eurjchem-1783	129	44	c	c	NOUN
eurjchem-1783	129	45	)	)	PUNCT
eurjchem-1783	129	46	,	,	PUNCT
eurjchem-1783	129	47	120.62	120.62	NUM
eurjchem-1783	129	48	(	(	PUNCT
eurjchem-1783	129	49	1c	1c	NOUN
eurjchem-1783	129	50	,	,	PUNCT
eurjchem-1783	129	51	ar	ar	NOUN
eurjchem-1783	129	52	-	-	NOUN
eurjchem-1783	129	53	c	c	NOUN
eurjchem-1783	129	54	)	)	PUNCT
eurjchem-1783	129	55	,	,	PUNCT
eurjchem-1783	129	56	117.0	117.0	NUM
eurjchem-1783	129	57	(	(	PUNCT
eurjchem-1783	129	58	1c	1c	NOUN
eurjchem-1783	129	59	,	,	PUNCT
eurjchem-1783	129	60	ar	ar	NOUN
eurjchem-1783	129	61	-	-	NOUN
eurjchem-1783	129	62	c	c	NOUN
eurjchem-1783	129	63	)	)	PUNCT
eurjchem-1783	129	64	,	,	PUNCT
eurjchem-1783	129	65	109.93	109.93	NUM
eurjchem-1783	129	66	(	(	PUNCT
eurjchem-1783	129	67	1c	1c	NOUN
eurjchem-1783	129	68	,	,	PUNCT
eurjchem-1783	129	69	ar	ar	NOUN
eurjchem-1783	129	70	-	-	NOUN
eurjchem-1783	129	71	c	c	NOUN
eurjchem-1783	129	72	)	)	PUNCT
eurjchem-1783	129	73	,	,	PUNCT
eurjchem-1783	129	74	85.0	85.0	NUM
eurjchem-1783	129	75	(	(	PUNCT
eurjchem-1783	129	76	1c	1c	X
eurjchem-1783	129	77	,	,	PUNCT
eurjchem-1783	129	78	ch	ch	NOUN
eurjchem-1783	129	79	)	)	PUNCT
eurjchem-1783	129	80	67.3	67.3	NUM
eurjchem-1783	129	81	(	(	PUNCT
eurjchem-1783	129	82	2c	2c	NOUN
eurjchem-1783	129	83	,	,	PUNCT
eurjchem-1783	129	84	ch2	ch2	PROPN
eurjchem-1783	129	85	)	)	PUNCT
eurjchem-1783	129	86	,	,	PUNCT
eurjchem-1783	129	87	50.3	50.3	NUM
eurjchem-1783	129	88	(	(	PUNCT
eurjchem-1783	129	89	2c	2c	NOUN
eurjchem-1783	129	90	,	,	PUNCT
eurjchem-1783	129	91	ch2	ch2	PROPN
eurjchem-1783	129	92	)	)	PUNCT
eurjchem-1783	129	93	,	,	PUNCT
eurjchem-1783	129	94	43.8	43.8	NUM
eurjchem-1783	129	95	(	(	PUNCT
eurjchem-1783	129	96	1c	1c	NOUN
eurjchem-1783	129	97	,	,	PUNCT
eurjchem-1783	129	98	ch2	ch2	PROPN
eurjchem-1783	129	99	)	)	PUNCT
eurjchem-1783	129	100	,	,	PUNCT
eurjchem-1783	129	101	31.2	31.2	NUM
eurjchem-1783	129	102	(	(	PUNCT
eurjchem-1783	129	103	1c	1c	NOUN
eurjchem-1783	129	104	,	,	PUNCT
eurjchem-1783	129	105	ch2br	ch2br	NOUN
eurjchem-1783	129	106	)	)	PUNCT
eurjchem-1783	129	107	.	.	PUNCT
eurjchem-1783	130	1	ms	ms	NOUN
eurjchem-1783	130	2	(	(	PUNCT
eurjchem-1783	130	3	m	m	PROPN
eurjchem-1783	130	4	/	/	SYM
eurjchem-1783	130	5	z	z	NOUN
eurjchem-1783	130	6	):	):	PUNCT
eurjchem-1783	130	7	359.1	359.1	NUM
eurjchem-1783	130	8	(	(	PUNCT
eurjchem-1783	130	9	m+	m+	NUM
eurjchem-1783	130	10	)	)	PUNCT
eurjchem-1783	130	11	.	.	PUNCT
eurjchem-1783	131	1	anal	anal	PROPN
eurjchem-1783	131	2	.	.	PUNCT
eurjchem-1783	131	3	calcd	calcd	NOUN
eurjchem-1783	131	4	.	.	PUNCT
eurjchem-1783	132	1	for	for	SCONJ
eurjchem-1783	132	2	c14h16brfn2o3	c14h16brfn2o3	PROPN
eurjchem-1783	132	3	:	:	PUNCT
eurjchem-1783	132	4	c	c	X
eurjchem-1783	132	5	,	,	PUNCT
eurjchem-1783	132	6	46.81	46.81	NUM
eurjchem-1783	132	7	;	;	PUNCT
eurjchem-1783	132	8	h	h	X
eurjchem-1783	132	9	,	,	PUNCT
eurjchem-1783	132	10	4.49	4.49	NUM
eurjchem-1783	132	11	;	;	PUNCT
eurjchem-1783	132	12	n	n	CCONJ
eurjchem-1783	132	13	,	,	PUNCT
eurjchem-1783	132	14	7.80	7.80	NUM
eurjchem-1783	132	15	.	.	PUNCT
eurjchem-1783	132	16	found	find	VERB
eurjchem-1783	132	17	:	:	PUNCT
eurjchem-1783	133	1	c	c	X
eurjchem-1783	133	2	,	,	PUNCT
eurjchem-1783	133	3	46.78	46.78	NUM
eurjchem-1783	133	4	;	;	PUNCT
eurjchem-1783	133	5	h	h	NOUN
eurjchem-1783	133	6	,	,	PUNCT
eurjchem-1783	133	7	4.25	4.25	NUM
eurjchem-1783	133	8	;	;	PUNCT
eurjchem-1783	133	9	n	n	CCONJ
eurjchem-1783	133	10	,	,	PUNCT
eurjchem-1783	133	11	7.82	7.82	NUM
eurjchem-1783	133	12	%	%	NOUN
eurjchem-1783	133	13	.	.	PUNCT
eurjchem-1783	134	1	2.2.5	2.2.5	X
eurjchem-1783	134	2	.	.	X
eurjchem-1783	135	1	synthesis	synthesis	NOUN
eurjchem-1783	135	2	of	of	ADP
eurjchem-1783	135	3	(	(	PUNCT
eurjchem-1783	135	4	s)-n-((3-(3	s)-n-((3-(3	PROPN
eurjchem-1783	135	5	-	-	PUNCT
eurjchem-1783	135	6	fluoro-4	fluoro-4	NOUN
eurjchem-1783	135	7	-	-	PUNCT
eurjchem-1783	135	8	morpholinophenyl)2	morpholinophenyl)2	NOUN
eurjchem-1783	135	9	-	-	PUNCT
eurjchem-1783	135	10	oxooxazolidin-5	oxooxazolidin-5	NUM
eurjchem-1783	135	11	-	-	PUNCT
eurjchem-1783	135	12	yl	yl	NOUN
eurjchem-1783	135	13	)	)	PUNCT
eurjchem-1783	135	14	methyl	methyl	NOUN
eurjchem-1783	135	15	)	)	PUNCT
eurjchem-1783	135	16	acetamide	acetamide	NOUN
eurjchem-1783	135	17	(	(	PUNCT
eurjchem-1783	135	18	5	5	NUM
eurjchem-1783	135	19	)	)	PUNCT
eurjchem-1783	135	20	(	(	PUNCT
eurjchem-1783	135	21	r)-5-(chloromethyl)-3-(3	r)-5-(chloromethyl)-3-(3	NOUN
eurjchem-1783	135	22	-	-	PUNCT
eurjchem-1783	135	23	fluoro-4	fluoro-4	NOUN
eurjchem-1783	135	24	-	-	PUNCT
eurjchem-1783	135	25	morpholinophenyl	morpholinophenyl	NOUN
eurjchem-1783	135	26	)	)	PUNCT
eurjchem-1783	135	27	oxazolidin-2	oxazolidin-2	NUM
eurjchem-1783	135	28	-	-	SYM
eurjchem-1783	135	29	one	one	NUM
eurjchem-1783	135	30	was	be	AUX
eurjchem-1783	135	31	dissolved	dissolve	VERB
eurjchem-1783	135	32	in	in	ADP
eurjchem-1783	135	33	dry	dry	ADJ
eurjchem-1783	135	34	acetonitrile	acetonitrile	NOUN
eurjchem-1783	135	35	(	(	PUNCT
eurjchem-1783	135	36	50	50	NUM
eurjchem-1783	135	37	ml	ml	NOUN
eurjchem-1783	135	38	)	)	PUNCT
eurjchem-1783	135	39	,	,	PUNCT
eurjchem-1783	135	40	added	add	VERB
eurjchem-1783	135	41	cesium	cesium	NOUN
eurjchem-1783	135	42	carbonate	carbonate	NOUN
eurjchem-1783	135	43	(	(	PUNCT
eurjchem-1783	135	44	5.91	5.91	NUM
eurjchem-1783	135	45	g	g	NOUN
eurjchem-1783	135	46	,	,	PUNCT
eurjchem-1783	135	47	0.018	0.018	NUM
eurjchem-1783	135	48	mol	mol	NOUN
eurjchem-1783	135	49	)	)	PUNCT
eurjchem-1783	135	50	,	,	PUNCT
eurjchem-1783	135	51	acetamide	acetamide	NOUN
eurjchem-1783	135	52	(	(	PUNCT
eurjchem-1783	135	53	0.71	0.71	NUM
eurjchem-1783	135	54	g	g	NOUN
eurjchem-1783	135	55	,	,	PUNCT
eurjchem-1783	135	56	0.013	0.013	NUM
eurjchem-1783	135	57	mol	mol	NOUN
eurjchem-1783	135	58	)	)	PUNCT
eurjchem-1783	135	59	and	and	CCONJ
eurjchem-1783	135	60	sodium	sodium	NOUN
eurjchem-1783	135	61	iodide	iodide	NOUN
eurjchem-1783	135	62	(	(	PUNCT
eurjchem-1783	135	63	0.181	0.181	NUM
eurjchem-1783	135	64	g	g	NOUN
eurjchem-1783	135	65	,	,	PUNCT
eurjchem-1783	135	66	0.0012	0.0012	NUM
eurjchem-1783	135	67	mol	mol	NOUN
eurjchem-1783	135	68	)	)	PUNCT
eurjchem-1783	135	69	,	,	PUNCT
eurjchem-1783	135	70	stirred	stir	VERB
eurjchem-1783	135	71	at	at	ADP
eurjchem-1783	135	72	room	room	NOUN
eurjchem-1783	135	73	temperature	temperature	NOUN
eurjchem-1783	135	74	for	for	ADP
eurjchem-1783	135	75	10	10	NUM
eurjchem-1783	135	76	min	min	NOUN
eurjchem-1783	135	77	and	and	CCONJ
eurjchem-1783	135	78	refluxed	refluxe	VERB
eurjchem-1783	135	79	for	for	ADP
eurjchem-1783	135	80	10	10	NUM
eurjchem-1783	135	81	hr	hr	NOUN
eurjchem-1783	135	82	.	.	PUNCT
eurjchem-1783	136	1	reaction	reaction	NOUN
eurjchem-1783	136	2	was	be	AUX
eurjchem-1783	136	3	monitored	monitor	VERB
eurjchem-1783	136	4	by	by	ADP
eurjchem-1783	136	5	tlc	tlc	NOUN
eurjchem-1783	136	6	.	.	PUNCT
eurjchem-1783	137	1	reaction	reaction	NOUN
eurjchem-1783	137	2	mixture	mixture	NOUN
eurjchem-1783	137	3	was	be	AUX
eurjchem-1783	137	4	cooled	cool	VERB
eurjchem-1783	137	5	,	,	PUNCT
eurjchem-1783	137	6	filtered	filter	VERB
eurjchem-1783	137	7	,	,	PUNCT
eurjchem-1783	137	8	concentrated	concentrate	VERB
eurjchem-1783	137	9	to	to	PART
eurjchem-1783	137	10	obtain	obtain	VERB
eurjchem-1783	137	11	crude	crude	ADJ
eurjchem-1783	137	12	compound	compound	NOUN
eurjchem-1783	137	13	which	which	PRON
eurjchem-1783	137	14	was	be	AUX
eurjchem-1783	137	15	further	far	ADV
eurjchem-1783	137	16	purified	purify	VERB
eurjchem-1783	137	17	by	by	ADP
eurjchem-1783	137	18	flash	flash	NOUN
eurjchem-1783	137	19	column	column	NOUN
eurjchem-1783	137	20	chromatography	chromatography	NOUN
eurjchem-1783	137	21	using	use	VERB
eurjchem-1783	137	22	1525	1525	NUM
eurjchem-1783	137	23	%	%	NOUN
eurjchem-1783	137	24	ethyl	ethyl	PROPN
eurjchem-1783	137	25	acetate	acetate	NOUN
eurjchem-1783	137	26	in	in	ADP
eurjchem-1783	137	27	hexane	hexane	NOUN
eurjchem-1783	137	28	to	to	PART
eurjchem-1783	137	29	obtain	obtain	VERB
eurjchem-1783	137	30	the	the	DET
eurjchem-1783	137	31	product	product	NOUN
eurjchem-1783	137	32	as	as	ADP
eurjchem-1783	137	33	white	white	ADJ
eurjchem-1783	137	34	color	color	NOUN
eurjchem-1783	137	35	solid	solid	ADJ
eurjchem-1783	137	36	(	(	PUNCT
eurjchem-1783	137	37	scheme	scheme	NOUN
eurjchem-1783	137	38	2	2	NUM
eurjchem-1783	137	39	)	)	PUNCT
eurjchem-1783	137	40	.	.	PUNCT
eurjchem-1783	138	1	color	color	NOUN
eurjchem-1783	138	2	:	:	PUNCT
eurjchem-1783	138	3	white	white	ADJ
eurjchem-1783	138	4	.	.	PUNCT
eurjchem-1783	139	1	yield	yield	NOUN
eurjchem-1783	139	2	:	:	PUNCT
eurjchem-1783	139	3	96	96	NUM
eurjchem-1783	139	4	%	%	NOUN
eurjchem-1783	139	5	.	.	PUNCT
eurjchem-1783	140	1	m.p	m.p	PROPN
eurjchem-1783	140	2	.	.	PROPN
eurjchem-1783	140	3	:	:	PUNCT
eurjchem-1783	141	1	180	180	NUM
eurjchem-1783	141	2	-	-	SYM
eurjchem-1783	141	3	182	182	NUM
eurjchem-1783	141	4	°	°	NUM
eurjchem-1783	141	5	c	c	NOUN
eurjchem-1783	141	6	.	.	PUNCT
eurjchem-1783	142	1	1h	1h	NUM
eurjchem-1783	142	2	nmr	nmr	NOUN
eurjchem-1783	142	3	(	(	PUNCT
eurjchem-1783	142	4	400	400	NUM
eurjchem-1783	142	5	mhz	mhz	NOUN
eurjchem-1783	142	6	,	,	PUNCT
eurjchem-1783	142	7	cdcl3	cdcl3	PROPN
eurjchem-1783	142	8	,	,	PUNCT
eurjchem-1783	142	9	δ	δ	PROPN
eurjchem-1783	142	10	,	,	PUNCT
eurjchem-1783	142	11	ppm	ppm	NOUN
eurjchem-1783	142	12	):	):	PUNCT
eurjchem-1783	142	13	7.34	7.34	NUM
eurjchem-1783	142	14	(	(	PUNCT
eurjchem-1783	142	15	dd	dd	PROPN
eurjchem-1783	142	16	,	,	PUNCT
eurjchem-1783	142	17	j	j	NOUN
eurjchem-1783	142	18	=	=	SYM
eurjchem-1783	142	19	4.2	4.2	NUM
eurjchem-1783	142	20	hz	hz	NOUN
eurjchem-1783	142	21	,	,	PUNCT
eurjchem-1783	142	22	2h	2h	NUM
eurjchem-1783	142	23	,	,	PUNCT
eurjchem-1783	142	24	ar	ar	NOUN
eurjchem-1783	142	25	-	-	NOUN
eurjchem-1783	142	26	h	h	NOUN
eurjchem-1783	142	27	)	)	PUNCT
eurjchem-1783	142	28	,	,	PUNCT
eurjchem-1783	142	29	6.86	6.86	NUM
eurjchem-1783	142	30	(	(	PUNCT
eurjchem-1783	142	31	dd	dd	PROPN
eurjchem-1783	142	32	,	,	PUNCT
eurjchem-1783	142	33	j	j	NOUN
eurjchem-1783	142	34	=	=	SYM
eurjchem-1783	142	35	4	4	NUM
eurjchem-1783	142	36	hz	hz	VERB
eurjchem-1783	142	37	,	,	PUNCT
eurjchem-1783	142	38	2	2	NUM
eurjchem-1783	142	39	hz	hz	NOUN
eurjchem-1783	142	40	,	,	PUNCT
eurjchem-1783	142	41	1h	1h	NUM
eurjchem-1783	142	42	,	,	PUNCT
eurjchem-1783	142	43	ar	ar	NOUN
eurjchem-1783	142	44	-	-	NOUN
eurjchem-1783	142	45	h	h	NOUN
eurjchem-1783	142	46	)	)	PUNCT
eurjchem-1783	142	47	,	,	PUNCT
eurjchem-1783	142	48	6.71	6.71	NUM
eurjchem-1783	142	49	(	(	PUNCT
eurjchem-1783	142	50	t	t	PROPN
eurjchem-1783	142	51	,	,	PUNCT
eurjchem-1783	142	52	j	j	PROPN
eurjchem-1783	143	1	=	=	SYM
eurjchem-1783	143	2	4	4	NUM
eurjchem-1783	143	3	hz	hz	NOUN
eurjchem-1783	143	4	,	,	PUNCT
eurjchem-1783	143	5	1h	1h	NUM
eurjchem-1783	143	6	,	,	PUNCT
eurjchem-1783	143	7	ar	ar	NOUN
eurjchem-1783	143	8	-	-	NOUN
eurjchem-1783	143	9	h	h	NOUN
eurjchem-1783	143	10	)	)	PUNCT
eurjchem-1783	143	11	,	,	PUNCT
eurjchem-1783	143	12	4.69	4.69	NUM
eurjchem-1783	143	13	(	(	PUNCT
eurjchem-1783	143	14	m	m	PROPN
eurjchem-1783	143	15	,	,	PUNCT
eurjchem-1783	143	16	1h	1h	NUM
eurjchem-1783	143	17	,	,	PUNCT
eurjchem-1783	143	18	ch	ch	NOUN
eurjchem-1783	143	19	)	)	PUNCT
eurjchem-1783	143	20	,	,	PUNCT
eurjchem-1783	143	21	3.79	3.79	NUM
eurjchem-1783	143	22	(	(	PUNCT
eurjchem-1783	143	23	t	t	PROPN
eurjchem-1783	143	24	,	,	PUNCT
eurjchem-1783	143	25	j	j	PROPN
eurjchem-1783	144	1	=	=	SYM
eurjchem-1783	144	2	5	5	NUM
eurjchem-1783	144	3	hz	hz	VERB
eurjchem-1783	144	4	,	,	PUNCT
eurjchem-1783	144	5	4h	4h	NOUN
eurjchem-1783	144	6	,	,	PUNCT
eurjchem-1783	144	7	morpholine	morpholine	ADJ
eurjchem-1783	144	8	-	-	PUNCT
eurjchem-1783	144	9	h	h	NOUN
eurjchem-1783	144	10	)	)	PUNCT
eurjchem-1783	144	11	,	,	PUNCT
eurjchem-1783	144	12	3.753.93	3.753.93	NUM
eurjchem-1783	144	13	(	(	PUNCT
eurjchem-1783	144	14	m	m	PROPN
eurjchem-1783	144	15	,	,	PUNCT
eurjchem-1783	144	16	2h	2h	NUM
eurjchem-1783	144	17	,	,	PUNCT
eurjchem-1783	144	18	ch2	ch2	PROPN
eurjchem-1783	144	19	)	)	PUNCT
eurjchem-1783	144	20	,	,	PUNCT
eurjchem-1783	144	21	3.56	3.56	NUM
eurjchem-1783	144	22	(	(	PUNCT
eurjchem-1783	144	23	m	m	PROPN
eurjchem-1783	144	24	,	,	PUNCT
eurjchem-1783	144	25	2h	2h	NUM
eurjchem-1783	144	26	,	,	PUNCT
eurjchem-1783	144	27	ch2	ch2	PROPN
eurjchem-1783	144	28	)	)	PUNCT
eurjchem-1783	144	29	,	,	PUNCT
eurjchem-1783	144	30	3.07	3.07	NUM
eurjchem-1783	144	31	(	(	PUNCT
eurjchem-1783	144	32	t	t	PROPN
eurjchem-1783	144	33	,	,	PUNCT
eurjchem-1783	144	34	j	j	PROPN
eurjchem-1783	145	1	=	=	SYM
eurjchem-1783	145	2	5	5	NUM
eurjchem-1783	145	3	hz	hz	VERB
eurjchem-1783	145	4	,	,	PUNCT
eurjchem-1783	145	5	4h	4h	NOUN
eurjchem-1783	145	6	,	,	PUNCT
eurjchem-1783	145	7	morpholine	morpholine	ADJ
eurjchem-1783	145	8	-	-	PUNCT
eurjchem-1783	145	9	h	h	NOUN
eurjchem-1783	145	10	)	)	PUNCT
eurjchem-1783	145	11	,	,	PUNCT
eurjchem-1783	145	12	1.99	1.99	NUM
eurjchem-1783	145	13	(	(	PUNCT
eurjchem-1783	145	14	s	s	PROPN
eurjchem-1783	145	15	,	,	PUNCT
eurjchem-1783	145	16	3h	3h	NUM
eurjchem-1783	145	17	,	,	PUNCT
eurjchem-1783	145	18	ch3	ch3	PROPN
eurjchem-1783	145	19	)	)	PUNCT
eurjchem-1783	145	20	.	.	PUNCT
eurjchem-1783	146	1	13c	13c	NOUN
eurjchem-1783	146	2	nmr	nmr	NOUN
eurjchem-1783	146	3	(	(	PUNCT
eurjchem-1783	146	4	100	100	NUM
eurjchem-1783	146	5	mhz	mhz	NOUN
eurjchem-1783	146	6	,	,	PUNCT
eurjchem-1783	146	7	cdcl3	cdcl3	PROPN
eurjchem-1783	146	8	,	,	PUNCT
eurjchem-1783	146	9	δ	δ	PROPN
eurjchem-1783	146	10	,	,	PUNCT
eurjchem-1783	146	11	ppm	ppm	NUM
eurjchem-1783	146	12	):	):	PUNCT
eurjchem-1783	146	13	171.4	171.4	NUM
eurjchem-1783	146	14	(	(	PUNCT
eurjchem-1783	146	15	1c	1c	NOUN
eurjchem-1783	146	16	,	,	PUNCT
eurjchem-1783	146	17	coch3	coch3	NOUN
eurjchem-1783	146	18	)	)	PUNCT
eurjchem-1783	146	19	,	,	PUNCT
eurjchem-1783	146	20	154.9	154.9	NUM
eurjchem-1783	146	21	(	(	PUNCT
eurjchem-1783	146	22	1c	1c	NOUN
eurjchem-1783	146	23	,	,	PUNCT
eurjchem-1783	146	24	co	co	NOUN
eurjchem-1783	146	25	)	)	PUNCT
eurjchem-1783	146	26	,	,	PUNCT
eurjchem-1783	146	27	148.1	148.1	NUM
eurjchem-1783	146	28	(	(	PUNCT
eurjchem-1783	146	29	1c	1c	NOUN
eurjchem-1783	146	30	,	,	PUNCT
eurjchem-1783	146	31	ar	ar	NOUN
eurjchem-1783	146	32	-	-	NOUN
eurjchem-1783	146	33	c	c	NOUN
eurjchem-1783	146	34	)	)	PUNCT
eurjchem-1783	146	35	,	,	PUNCT
eurjchem-1783	146	36	135.3	135.3	NUM
eurjchem-1783	146	37	(	(	PUNCT
eurjchem-1783	146	38	1c	1c	NOUN
eurjchem-1783	146	39	,	,	PUNCT
eurjchem-1783	146	40	ar	ar	NOUN
eurjchem-1783	146	41	-	-	NOUN
eurjchem-1783	146	42	c	c	NOUN
eurjchem-1783	146	43	)	)	PUNCT
eurjchem-1783	146	44	,	,	PUNCT
eurjchem-1783	146	45	130.2	130.2	NUM
eurjchem-1783	146	46	(	(	PUNCT
eurjchem-1783	146	47	1c	1c	NOUN
eurjchem-1783	146	48	,	,	PUNCT
eurjchem-1783	146	49	ar	ar	NOUN
eurjchem-1783	146	50	-	-	NOUN
eurjchem-1783	146	51	c	c	NOUN
eurjchem-1783	146	52	)	)	PUNCT
eurjchem-1783	146	53	,	,	PUNCT
eurjchem-1783	146	54	119.3	119.3	NUM
eurjchem-1783	146	55	(	(	PUNCT
eurjchem-1783	146	56	2c	2c	NUM
eurjchem-1783	146	57	,	,	PUNCT
eurjchem-1783	146	58	ar	ar	NOUN
eurjchem-1783	146	59	-	-	NOUN
eurjchem-1783	146	60	c	c	NOUN
eurjchem-1783	146	61	)	)	PUNCT
eurjchem-1783	146	62	,	,	PUNCT
eurjchem-1783	146	63	115.9	115.9	NUM
eurjchem-1783	146	64	(	(	PUNCT
eurjchem-1783	146	65	2c	2c	NUM
eurjchem-1783	146	66	,	,	PUNCT
eurjchem-1783	146	67	ar	ar	NOUN
eurjchem-1783	146	68	-	-	NOUN
eurjchem-1783	146	69	c	c	NOUN
eurjchem-1783	146	70	)	)	PUNCT
eurjchem-1783	146	71	,	,	PUNCT
eurjchem-1783	146	72	71.9	71.9	NUM
eurjchem-1783	146	73	(	(	PUNCT
eurjchem-1783	146	74	1c	1c	X
eurjchem-1783	146	75	,	,	PUNCT
eurjchem-1783	146	76	ch	ch	NOUN
eurjchem-1783	146	77	)	)	PUNCT
eurjchem-1783	146	78	,	,	PUNCT
eurjchem-1783	146	79	66.6	66.6	NUM
eurjchem-1783	146	80	(	(	PUNCT
eurjchem-1783	146	81	2c	2c	NUM
eurjchem-1783	146	82	,	,	PUNCT
eurjchem-1783	146	83	ch2	ch2	PROPN
eurjchem-1783	146	84	)	)	PUNCT
eurjchem-1783	146	85	,	,	PUNCT
eurjchem-1783	146	86	49.3	49.3	NUM
eurjchem-1783	146	87	(	(	PUNCT
eurjchem-1783	146	88	2c	2c	NOUN
eurjchem-1783	146	89	,	,	PUNCT
eurjchem-1783	146	90	ch2	ch2	PROPN
eurjchem-1783	146	91	)	)	PUNCT
eurjchem-1783	146	92	,	,	PUNCT
eurjchem-1783	146	93	47.8	47.8	NUM
eurjchem-1783	146	94	(	(	PUNCT
eurjchem-1783	146	95	1c	1c	NOUN
eurjchem-1783	146	96	,	,	PUNCT
eurjchem-1783	146	97	ch2	ch2	PROPN
eurjchem-1783	146	98	)	)	PUNCT
eurjchem-1783	146	99	,	,	PUNCT
eurjchem-1783	146	100	41.73	41.73	NUM
eurjchem-1783	146	101	(	(	PUNCT
eurjchem-1783	146	102	1c	1c	NOUN
eurjchem-1783	146	103	,	,	PUNCT
eurjchem-1783	146	104	ch2	ch2	PROPN
eurjchem-1783	146	105	)	)	PUNCT
eurjchem-1783	146	106	,	,	PUNCT
eurjchem-1783	146	107	22.74	22.74	NUM
eurjchem-1783	146	108	(	(	PUNCT
eurjchem-1783	146	109	1c	1c	NOUN
eurjchem-1783	146	110	,	,	PUNCT
eurjchem-1783	146	111	ch3	ch3	PROPN
eurjchem-1783	146	112	)	)	PUNCT
eurjchem-1783	146	113	.	.	PUNCT
eurjchem-1783	147	1	ms	ms	NOUN
eurjchem-1783	147	2	(	(	PUNCT
eurjchem-1783	147	3	m	m	PROPN
eurjchem-1783	147	4	/	/	SYM
eurjchem-1783	147	5	z	z	NOUN
eurjchem-1783	147	6	):	):	PUNCT
eurjchem-1783	147	7	338.2	338.2	NUM
eurjchem-1783	147	8	(	(	PUNCT
eurjchem-1783	147	9	m+	m+	NUM
eurjchem-1783	147	10	)	)	PUNCT
eurjchem-1783	147	11	.	.	PUNCT
eurjchem-1783	148	1	anal	anal	PROPN
eurjchem-1783	148	2	.	.	PUNCT
eurjchem-1783	148	3	calcd	calcd	NOUN
eurjchem-1783	148	4	.	.	PUNCT
eurjchem-1783	149	1	for	for	ADP
eurjchem-1783	149	2	c16h20fn3o4	c16h20fn3o4	NOUN
eurjchem-1783	149	3	:	:	PUNCT
eurjchem-1783	149	4	c	c	X
eurjchem-1783	149	5	,	,	PUNCT
eurjchem-1783	149	6	56.97	56.97	NUM
eurjchem-1783	149	7	;	;	PUNCT
eurjchem-1783	149	8	h	h	NOUN
eurjchem-1783	149	9	,	,	PUNCT
eurjchem-1783	149	10	5.98	5.98	NUM
eurjchem-1783	149	11	;	;	PUNCT
eurjchem-1783	149	12	n	n	CCONJ
eurjchem-1783	149	13	,	,	PUNCT
eurjchem-1783	149	14	12.46	12.46	NUM
eurjchem-1783	149	15	.	.	PUNCT
eurjchem-1783	149	16	found	find	VERB
eurjchem-1783	149	17	:	:	PUNCT
eurjchem-1783	150	1	c	c	X
eurjchem-1783	150	2	,	,	PUNCT
eurjchem-1783	150	3	56.75	56.75	NUM
eurjchem-1783	150	4	;	;	PUNCT
eurjchem-1783	150	5	h	h	NOUN
eurjchem-1783	150	6	,	,	PUNCT
eurjchem-1783	150	7	6.08	6.08	NUM
eurjchem-1783	150	8	;	;	PUNCT
eurjchem-1783	150	9	n	n	CCONJ
eurjchem-1783	150	10	,	,	PUNCT
eurjchem-1783	150	11	12.01	12.01	NUM
eurjchem-1783	150	12	%	%	NOUN
eurjchem-1783	150	13	.	.	PUNCT
eurjchem-1783	151	1	2018	2018	NUM
eurjchem-1783	151	2	–	–	PUNCT
eurjchem-1783	151	3	european	european	ADJ
eurjchem-1783	151	4	journal	journal	NOUN
eurjchem-1783	151	5	of	of	ADP
eurjchem-1783	151	6	chemistry	chemistry	NOUN
eurjchem-1783	151	7	–	–	PUNCT
eurjchem-1783	151	8	cc	cc	NOUN
eurjchem-1783	151	9	by	by	ADP
eurjchem-1783	151	10	nc	nc	PROPN
eurjchem-1783	151	11	–	–	PUNCT
eurjchem-1783	151	12	doi	doi	PROPN
eurjchem-1783	151	13	:	:	PUNCT
eurjchem-1783	151	14	10.5155	10.5155	NUM
eurjchem-1783	151	15	/	/	SYM
eurjchem-1783	151	16	eurjchem.9.4.353	eurjchem.9.4.353	PROPN
eurjchem-1783	151	17	-	-	PUNCT
eurjchem-1783	151	18	359.1783	359.1783	NUM
eurjchem-1783	151	19	356	356	NUM
eurjchem-1783	151	20	siddaraj	siddaraj	ADJ
eurjchem-1783	151	21	et	et	NOUN
eurjchem-1783	151	22	al	al	PROPN
eurjchem-1783	151	23	.	.	PUNCT
eurjchem-1783	151	24	/	/	SYM
eurjchem-1783	151	25	european	european	PROPN
eurjchem-1783	151	26	journal	journal	PROPN
eurjchem-1783	151	27	of	of	ADP
eurjchem-1783	151	28	chemistry	chemistry	NOUN
eurjchem-1783	151	29	9	9	NUM
eurjchem-1783	151	30	(	(	PUNCT
eurjchem-1783	151	31	4	4	NUM
eurjchem-1783	151	32	)	)	PUNCT
eurjchem-1783	151	33	(	(	PUNCT
eurjchem-1783	151	34	2018	2018	NUM
eurjchem-1783	151	35	)	)	PUNCT
eurjchem-1783	151	36	353	353	NUM
eurjchem-1783	151	37	-	-	SYM
eurjchem-1783	151	38	359	359	NUM
eurjchem-1783	151	39	n	n	NUM
eurjchem-1783	151	40	h	h	NOUN
eurjchem-1783	151	41	h	h	NOUN
eurjchem-1783	152	1	n	n	PROPN
eurjchem-1783	152	2	f	f	PROPN
eurjchem-1783	152	3	f	f	PROPN
eurjchem-1783	152	4	no2	no2	PROPN
eurjchem-1783	152	5	n	n	CCONJ
eurjchem-1783	152	6	h	h	NOUN
eurjchem-1783	153	1	n	n	CCONJ
eurjchem-1783	154	1	f	f	PROPN
eurjchem-1783	154	2	no2	no2	PROPN
eurjchem-1783	154	3	n	n	CCONJ
eurjchem-1783	154	4	n	n	PROPN
eurjchem-1783	154	5	f	f	PROPN
eurjchem-1783	154	6	no2	no2	NOUN
eurjchem-1783	154	7	boc	boc	NOUN
eurjchem-1783	154	8	n	n	CCONJ
eurjchem-1783	154	9	n	n	NOUN
eurjchem-1783	154	10	f	f	NOUN
eurjchem-1783	154	11	nh2	nh2	PROPN
eurjchem-1783	154	12	boc	boc	VERB
eurjchem-1783	154	13	6	6	NUM
eurjchem-1783	154	14	7	7	NUM
eurjchem-1783	154	15	8	8	NUM
eurjchem-1783	154	16	n	n	ADP
eurjchem-1783	154	17	n	n	NOUN
eurjchem-1783	154	18	f	f	NOUN
eurjchem-1783	154	19	hn	hn	PROPN
eurjchem-1783	154	20	boc	boc	NOUN
eurjchem-1783	154	21	o	o	NOUN
eurjchem-1783	154	22	o	o	NOUN
eurjchem-1783	154	23	n	n	CCONJ
eurjchem-1783	154	24	n	n	PROPN
eurjchem-1783	154	25	f	f	NOUN
eurjchem-1783	154	26	n	n	ADV
eurjchem-1783	154	27	boc	boc	VERB
eurjchem-1783	155	1	o	o	NOUN
eurjchem-1783	156	1	o	o	NOUN
eurjchem-1783	157	1	br	br	NOUN
eurjchem-1783	158	1	a	a	DET
eurjchem-1783	158	2	b	b	NOUN
eurjchem-1783	158	3	c	c	NOUN
eurjchem-1783	158	4	d	d	PROPN
eurjchem-1783	158	5	e	e	PROPN
eurjchem-1783	158	6	9	9	NUM
eurjchem-1783	158	7	10	10	NUM
eurjchem-1783	158	8	n	n	CCONJ
eurjchem-1783	158	9	n	n	NOUN
eurjchem-1783	158	10	f	f	NOUN
eurjchem-1783	158	11	n	n	ADV
eurjchem-1783	158	12	boc	boc	VERB
eurjchem-1783	158	13	o	o	NOUN
eurjchem-1783	158	14	o	o	NOUN
eurjchem-1783	159	1	hn	hn	INTJ
eurjchem-1783	159	2	o	o	X
eurjchem-1783	159	3	f	f	PROPN
eurjchem-1783	159	4	11	11	NUM
eurjchem-1783	159	5	g	g	PROPN
eurjchem-1783	159	6	n	n	PRON
eurjchem-1783	159	7	h	h	NOUN
eurjchem-1783	160	1	n	n	NOUN
eurjchem-1783	160	2	f	f	PROPN
eurjchem-1783	160	3	n	n	ADV
eurjchem-1783	161	1	o	o	NOUN
eurjchem-1783	161	2	o	o	X
eurjchem-1783	162	1	hn	hn	NOUN
eurjchem-1783	162	2	o	o	NOUN
eurjchem-1783	162	3	12	12	NUM
eurjchem-1783	162	4	h	h	NOUN
eurjchem-1783	162	5	n	n	ADP
eurjchem-1783	162	6	n	n	NOUN
eurjchem-1783	162	7	f	f	PROPN
eurjchem-1783	162	8	n	n	ADV
eurjchem-1783	163	1	o	o	NOUN
eurjchem-1783	164	1	o	o	X
eurjchem-1783	164	2	hn	hn	NOUN
eurjchem-1783	164	3	o	o	NOUN
eurjchem-1783	165	1	13	13	NUM
eurjchem-1783	165	2	o	o	NOUN
eurjchem-1783	165	3	oh	oh	INTJ
eurjchem-1783	165	4	eperezolid	eperezolid	NOUN
eurjchem-1783	165	5	reagents	reagent	NOUN
eurjchem-1783	165	6	and	and	CCONJ
eurjchem-1783	165	7	conditions	condition	NOUN
eurjchem-1783	165	8	:	:	PUNCT
eurjchem-1783	165	9	a	a	X
eurjchem-1783	165	10	)	)	PUNCT
eurjchem-1783	165	11	tea	tea	NOUN
eurjchem-1783	165	12	,	,	PUNCT
eurjchem-1783	165	13	thf	thf	NOUN
eurjchem-1783	165	14	;	;	PUNCT
eurjchem-1783	165	15	b	b	X
eurjchem-1783	165	16	)	)	PUNCT
eurjchem-1783	165	17	boc	boc	NOUN
eurjchem-1783	165	18	anhydride	anhydride	NOUN
eurjchem-1783	165	19	,	,	PUNCT
eurjchem-1783	165	20	tea	tea	NOUN
eurjchem-1783	165	21	,	,	PUNCT
eurjchem-1783	165	22	dcm	dcm	PROPN
eurjchem-1783	165	23	;	;	PUNCT
eurjchem-1783	165	24	c	c	X
eurjchem-1783	165	25	)	)	PUNCT
eurjchem-1783	165	26	raney	raney	PROPN
eurjchem-1783	165	27	ni	ni	PROPN
eurjchem-1783	165	28	,	,	PUNCT
eurjchem-1783	165	29	nh2nh2	nh2nh2	NOUN
eurjchem-1783	165	30	,	,	PUNCT
eurjchem-1783	165	31	etoh	etoh	NOUN
eurjchem-1783	165	32	;	;	PUNCT
eurjchem-1783	165	33	d	d	X
eurjchem-1783	165	34	)	)	PUNCT
eurjchem-1783	165	35	cbz	cbz	NOUN
eurjchem-1783	165	36	-	-	PUNCT
eurjchem-1783	165	37	cl	cl	NOUN
eurjchem-1783	165	38	,	,	PUNCT
eurjchem-1783	165	39	tea	tea	NOUN
eurjchem-1783	165	40	,	,	PUNCT
eurjchem-1783	165	41	thf	thf	NOUN
eurjchem-1783	165	42	;	;	PUNCT
eurjchem-1783	165	43	e	e	X
eurjchem-1783	165	44	)	)	PUNCT
eurjchem-1783	165	45	2-(bromomethyl)oxirane	2-(bromomethyl)oxirane	NUM
eurjchem-1783	165	46	,	,	PUNCT
eurjchem-1783	165	47	csco3	csco3	ADJ
eurjchem-1783	165	48	,	,	PUNCT
eurjchem-1783	165	49	ch3cn	ch3cn	NUM
eurjchem-1783	165	50	;	;	PUNCT
eurjchem-1783	165	51	f	f	X
eurjchem-1783	165	52	)	)	PUNCT
eurjchem-1783	165	53	acetamide	acetamide	NOUN
eurjchem-1783	165	54	,	,	PUNCT
eurjchem-1783	165	55	csco3	csco3	PROPN
eurjchem-1783	165	56	,	,	PUNCT
eurjchem-1783	165	57	nai	nai	PROPN
eurjchem-1783	165	58	,	,	PUNCT
eurjchem-1783	165	59	ch3cn	ch3cn	NUM
eurjchem-1783	165	60	;	;	PUNCT
eurjchem-1783	165	61	g	g	NOUN
eurjchem-1783	165	62	)	)	PUNCT
eurjchem-1783	165	63	hcl	hcl	PROPN
eurjchem-1783	165	64	in	in	ADP
eurjchem-1783	165	65	ether	ether	NOUN
eurjchem-1783	165	66	;	;	PUNCT
eurjchem-1783	165	67	h	h	X
eurjchem-1783	165	68	)	)	PUNCT
eurjchem-1783	165	69	edci	edci	PROPN
eurjchem-1783	165	70	.	.	PUNCT
eurjchem-1783	166	1	hobt	hobt	ADJ
eurjchem-1783	166	2	,	,	PUNCT
eurjchem-1783	166	3	tea	tea	NOUN
eurjchem-1783	166	4	,	,	PUNCT
eurjchem-1783	166	5	dcm	dcm	PROPN
eurjchem-1783	166	6	.	.	PROPN
eurjchem-1783	166	7	scheme	scheme	PROPN
eurjchem-1783	166	8	3	3	NUM
eurjchem-1783	166	9	2.2.6	2.2.6	NUM
eurjchem-1783	166	10	.	.	PUNCT
eurjchem-1783	167	1	synthesis	synthesis	NOUN
eurjchem-1783	167	2	of	of	ADP
eurjchem-1783	167	3	1-(2	1-(2	PROPN
eurjchem-1783	167	4	-	-	PUNCT
eurjchem-1783	167	5	fluoro-4	fluoro-4	NOUN
eurjchem-1783	167	6	-	-	PUNCT
eurjchem-1783	167	7	nitrophenyl	nitrophenyl	NOUN
eurjchem-1783	167	8	)	)	PUNCT
eurjchem-1783	167	9	piperazine	piperazine	NOUN
eurjchem-1783	167	10	(	(	PUNCT
eurjchem-1783	167	11	6	6	NUM
eurjchem-1783	167	12	)	)	PUNCT
eurjchem-1783	167	13	3,4	3,4	NUM
eurjchem-1783	167	14	-	-	NUM
eurjchem-1783	167	15	difluoronitrobenzene	difluoronitrobenzene	NOUN
eurjchem-1783	167	16	(	(	PUNCT
eurjchem-1783	167	17	25	25	NUM
eurjchem-1783	167	18	g	g	NOUN
eurjchem-1783	167	19	,	,	PUNCT
eurjchem-1783	167	20	0.157	0.157	NUM
eurjchem-1783	167	21	mol	mol	NOUN
eurjchem-1783	167	22	)	)	PUNCT
eurjchem-1783	167	23	was	be	AUX
eurjchem-1783	167	24	dissolved	dissolve	VERB
eurjchem-1783	167	25	in	in	ADP
eurjchem-1783	167	26	250	250	NUM
eurjchem-1783	167	27	ml	ml	NOUN
eurjchem-1783	167	28	of	of	ADP
eurjchem-1783	167	29	dry	dry	ADJ
eurjchem-1783	167	30	thf	thf	NOUN
eurjchem-1783	167	31	at	at	ADP
eurjchem-1783	167	32	room	room	NOUN
eurjchem-1783	167	33	temperature	temperature	NOUN
eurjchem-1783	167	34	,	,	PUNCT
eurjchem-1783	167	35	added	add	VERB
eurjchem-1783	167	36	piperazine	piperazine	NOUN
eurjchem-1783	167	37	(	(	PUNCT
eurjchem-1783	167	38	14.20	14.20	NUM
eurjchem-1783	167	39	g	g	NOUN
eurjchem-1783	167	40	,	,	PUNCT
eurjchem-1783	167	41	0.165	0.165	NUM
eurjchem-1783	167	42	mol	mol	NOUN
eurjchem-1783	167	43	)	)	PUNCT
eurjchem-1783	167	44	and	and	CCONJ
eurjchem-1783	167	45	triethyl	triethyl	PROPN
eurjchem-1783	167	46	amine	amine	PROPN
eurjchem-1783	167	47	(	(	PUNCT
eurjchem-1783	167	48	26.18	26.18	NUM
eurjchem-1783	167	49	ml	ml	NOUN
eurjchem-1783	167	50	,	,	PUNCT
eurjchem-1783	167	51	0.188	0.188	NUM
eurjchem-1783	167	52	mol	mol	NOUN
eurjchem-1783	167	53	)	)	PUNCT
eurjchem-1783	167	54	very	very	ADV
eurjchem-1783	167	55	slowly	slowly	ADV
eurjchem-1783	167	56	at	at	ADP
eurjchem-1783	167	57	room	room	NOUN
eurjchem-1783	167	58	temperature	temperature	NOUN
eurjchem-1783	167	59	and	and	CCONJ
eurjchem-1783	167	60	stirred	stir	VERB
eurjchem-1783	167	61	at	at	ADP
eurjchem-1783	167	62	the	the	DET
eurjchem-1783	167	63	same	same	ADJ
eurjchem-1783	167	64	for	for	ADP
eurjchem-1783	167	65	15	15	NUM
eurjchem-1783	167	66	mins	min	NOUN
eurjchem-1783	167	67	.	.	PUNCT
eurjchem-1783	168	1	reaction	reaction	NOUN
eurjchem-1783	168	2	mixture	mixture	NOUN
eurjchem-1783	168	3	was	be	AUX
eurjchem-1783	168	4	heated	heat	VERB
eurjchem-1783	168	5	to	to	ADP
eurjchem-1783	168	6	60	60	NUM
eurjchem-1783	168	7	°	°	NOUN
eurjchem-1783	168	8	c	c	NOUN
eurjchem-1783	168	9	for	for	ADP
eurjchem-1783	168	10	2	2	NUM
eurjchem-1783	168	11	hr	hr	NOUN
eurjchem-1783	168	12	.	.	PUNCT
eurjchem-1783	169	1	completion	completion	NOUN
eurjchem-1783	169	2	of	of	ADP
eurjchem-1783	169	3	the	the	DET
eurjchem-1783	169	4	reaction	reaction	NOUN
eurjchem-1783	169	5	was	be	AUX
eurjchem-1783	169	6	monitored	monitor	VERB
eurjchem-1783	169	7	by	by	ADP
eurjchem-1783	169	8	tlc	tlc	PROPN
eurjchem-1783	169	9	.	.	PUNCT
eurjchem-1783	170	1	after	after	ADP
eurjchem-1783	170	2	the	the	DET
eurjchem-1783	170	3	completion	completion	NOUN
eurjchem-1783	170	4	of	of	ADP
eurjchem-1783	170	5	the	the	DET
eurjchem-1783	170	6	reaction	reaction	NOUN
eurjchem-1783	170	7	,	,	PUNCT
eurjchem-1783	170	8	added	add	VERB
eurjchem-1783	170	9	100	100	NUM
eurjchem-1783	170	10	ml	ml	NOUN
eurjchem-1783	170	11	of	of	ADP
eurjchem-1783	170	12	water	water	NOUN
eurjchem-1783	170	13	and	and	CCONJ
eurjchem-1783	170	14	500	500	NUM
eurjchem-1783	170	15	ml	ml	NOUN
eurjchem-1783	170	16	of	of	ADP
eurjchem-1783	170	17	ethyl	ethyl	PROPN
eurjchem-1783	170	18	acetate	acetate	PROPN
eurjchem-1783	170	19	into	into	ADP
eurjchem-1783	170	20	the	the	DET
eurjchem-1783	170	21	reaction	reaction	NOUN
eurjchem-1783	170	22	mixture	mixture	NOUN
eurjchem-1783	170	23	,	,	PUNCT
eurjchem-1783	170	24	organic	organic	ADJ
eurjchem-1783	170	25	layer	layer	NOUN
eurjchem-1783	170	26	was	be	AUX
eurjchem-1783	170	27	separated	separate	VERB
eurjchem-1783	170	28	,	,	PUNCT
eurjchem-1783	170	29	aqueous	aqueous	ADJ
eurjchem-1783	170	30	layer	layer	NOUN
eurjchem-1783	170	31	was	be	AUX
eurjchem-1783	170	32	extracted	extract	VERB
eurjchem-1783	170	33	with	with	ADP
eurjchem-1783	170	34	(	(	PUNCT
eurjchem-1783	170	35	250	250	NUM
eurjchem-1783	170	36	ml	ml	NOUN
eurjchem-1783	170	37	×	×	PROPN
eurjchem-1783	170	38	2	2	NUM
eurjchem-1783	170	39	)	)	PUNCT
eurjchem-1783	170	40	,	,	PUNCT
eurjchem-1783	170	41	and	and	CCONJ
eurjchem-1783	170	42	combined	combined	ADJ
eurjchem-1783	170	43	organic	organic	ADJ
eurjchem-1783	170	44	layers	layer	NOUN
eurjchem-1783	170	45	were	be	AUX
eurjchem-1783	170	46	washed	wash	VERB
eurjchem-1783	170	47	with	with	ADP
eurjchem-1783	170	48	water	water	NOUN
eurjchem-1783	170	49	(	(	PUNCT
eurjchem-1783	170	50	100	100	NUM
eurjchem-1783	170	51	ml	ml	NOUN
eurjchem-1783	170	52	×	×	PROPN
eurjchem-1783	170	53	2	2	NUM
eurjchem-1783	170	54	)	)	PUNCT
eurjchem-1783	170	55	,	,	PUNCT
eurjchem-1783	170	56	brine	brine	NOUN
eurjchem-1783	170	57	(	(	PUNCT
eurjchem-1783	170	58	100	100	NUM
eurjchem-1783	170	59	ml	ml	PART
eurjchem-1783	170	60	×	×	PROPN
eurjchem-1783	170	61	1	1	NUM
eurjchem-1783	170	62	)	)	PUNCT
eurjchem-1783	170	63	,	,	PUNCT
eurjchem-1783	170	64	dried	dry	VERB
eurjchem-1783	170	65	over	over	ADP
eurjchem-1783	170	66	na2so4	na2so4	NOUN
eurjchem-1783	170	67	and	and	CCONJ
eurjchem-1783	170	68	concentrated	concentrate	VERB
eurjchem-1783	170	69	to	to	PART
eurjchem-1783	170	70	give	give	VERB
eurjchem-1783	170	71	crude	crude	ADJ
eurjchem-1783	170	72	product	product	NOUN
eurjchem-1783	170	73	.	.	PUNCT
eurjchem-1783	171	1	crude	crude	ADJ
eurjchem-1783	171	2	product	product	NOUN
eurjchem-1783	171	3	obtained	obtain	VERB
eurjchem-1783	171	4	was	be	AUX
eurjchem-1783	171	5	added	add	VERB
eurjchem-1783	171	6	diethyl	diethyl	NOUN
eurjchem-1783	171	7	ether	ether	NOUN
eurjchem-1783	171	8	(	(	PUNCT
eurjchem-1783	171	9	100	100	NUM
eurjchem-1783	171	10	ml	ml	PART
eurjchem-1783	171	11	×	×	PROPN
eurjchem-1783	171	12	2	2	NUM
eurjchem-1783	171	13	)	)	PUNCT
eurjchem-1783	171	14	and	and	CCONJ
eurjchem-1783	171	15	stirred	stir	VERB
eurjchem-1783	171	16	at	at	ADP
eurjchem-1783	171	17	room	room	NOUN
eurjchem-1783	171	18	temperature	temperature	NOUN
eurjchem-1783	171	19	,	,	PUNCT
eurjchem-1783	171	20	filtered	filter	VERB
eurjchem-1783	171	21	and	and	CCONJ
eurjchem-1783	171	22	dried	dry	VERB
eurjchem-1783	171	23	to	to	PART
eurjchem-1783	171	24	afford	afford	VERB
eurjchem-1783	171	25	a	a	DET
eurjchem-1783	171	26	product	product	NOUN
eurjchem-1783	171	27	as	as	ADP
eurjchem-1783	171	28	brown	brown	ADJ
eurjchem-1783	171	29	solid	solid	ADJ
eurjchem-1783	171	30	(	(	PUNCT
eurjchem-1783	171	31	scheme	scheme	NOUN
eurjchem-1783	171	32	3	3	NUM
eurjchem-1783	171	33	)	)	PUNCT
eurjchem-1783	171	34	.	.	PUNCT
eurjchem-1783	172	1	color	color	NOUN
eurjchem-1783	172	2	:	:	PUNCT
eurjchem-1783	172	3	brown	brown	ADJ
eurjchem-1783	172	4	.	.	PUNCT
eurjchem-1783	173	1	yield	yield	NOUN
eurjchem-1783	173	2	:	:	PUNCT
eurjchem-1783	173	3	99	99	NUM
eurjchem-1783	173	4	%	%	NOUN
eurjchem-1783	173	5	.	.	PUNCT
eurjchem-1783	174	1	m.p	m.p	PROPN
eurjchem-1783	174	2	.	.	PROPN
eurjchem-1783	174	3	:	:	PUNCT
eurjchem-1783	175	1	68	68	NUM
eurjchem-1783	175	2	-	-	SYM
eurjchem-1783	175	3	69	69	NUM
eurjchem-1783	175	4	°	°	NUM
eurjchem-1783	175	5	c	c	NOUN
eurjchem-1783	175	6	.	.	PUNCT
eurjchem-1783	176	1	1h	1h	NUM
eurjchem-1783	176	2	nmr	nmr	NOUN
eurjchem-1783	176	3	(	(	PUNCT
eurjchem-1783	176	4	400	400	NUM
eurjchem-1783	176	5	mhz	mhz	NOUN
eurjchem-1783	176	6	,	,	PUNCT
eurjchem-1783	176	7	cdcl3	cdcl3	PROPN
eurjchem-1783	176	8	,	,	PUNCT
eurjchem-1783	176	9	δ	δ	PROPN
eurjchem-1783	176	10	,	,	PUNCT
eurjchem-1783	176	11	ppm	ppm	NUM
eurjchem-1783	176	12	):	):	PUNCT
eurjchem-1783	176	13	8.01	8.01	NUM
eurjchem-1783	176	14	-	-	SYM
eurjchem-1783	176	15	7.98	7.98	NUM
eurjchem-1783	176	16	(	(	PUNCT
eurjchem-1783	176	17	dd	dd	NOUN
eurjchem-1783	176	18	,	,	PUNCT
eurjchem-1783	176	19	j	j	PROPN
eurjchem-1783	177	1	=	=	SYM
eurjchem-1783	177	2	2.25	2.25	NUM
eurjchem-1783	177	3	hz	hz	NOUN
eurjchem-1783	177	4	,	,	PUNCT
eurjchem-1783	177	5	1h	1h	NUM
eurjchem-1783	177	6	,	,	PUNCT
eurjchem-1783	177	7	ar	ar	NOUN
eurjchem-1783	177	8	-	-	NOUN
eurjchem-1783	177	9	h	h	NOUN
eurjchem-1783	177	10	)	)	PUNCT
eurjchem-1783	177	11	,	,	PUNCT
eurjchem-1783	177	12	7.90	7.90	NUM
eurjchem-1783	177	13	(	(	PUNCT
eurjchem-1783	177	14	dd	dd	PROPN
eurjchem-1783	177	15	,	,	PUNCT
eurjchem-1783	177	16	j	j	PROPN
eurjchem-1783	178	1	=	=	SYM
eurjchem-1783	178	2	12.92	12.92	NUM
eurjchem-1783	178	3	hz	hz	NOUN
eurjchem-1783	178	4	,	,	PUNCT
eurjchem-1783	178	5	1h	1h	NUM
eurjchem-1783	178	6	,	,	PUNCT
eurjchem-1783	178	7	ar	ar	NOUN
eurjchem-1783	178	8	-	-	NOUN
eurjchem-1783	178	9	h	h	NOUN
eurjchem-1783	178	10	)	)	PUNCT
eurjchem-1783	178	11	,	,	PUNCT
eurjchem-1783	178	12	6.94	6.94	NUM
eurjchem-1783	178	13	(	(	PUNCT
eurjchem-1783	178	14	t	t	PROPN
eurjchem-1783	178	15	,	,	PUNCT
eurjchem-1783	178	16	j	j	PROPN
eurjchem-1783	179	1	=	=	PROPN
eurjchem-1783	179	2	8.72	8.72	NUM
eurjchem-1783	179	3	hz	hz	NOUN
eurjchem-1783	179	4	,	,	PUNCT
eurjchem-1783	179	5	1h	1h	NUM
eurjchem-1783	179	6	,	,	PUNCT
eurjchem-1783	179	7	ar	ar	NOUN
eurjchem-1783	179	8	-	-	NOUN
eurjchem-1783	179	9	h	h	NOUN
eurjchem-1783	179	10	)	)	PUNCT
eurjchem-1783	179	11	,	,	PUNCT
eurjchem-1783	179	12	3.12	3.12	NUM
eurjchem-1783	179	13	(	(	PUNCT
eurjchem-1783	179	14	t	t	PROPN
eurjchem-1783	179	15	,	,	PUNCT
eurjchem-1783	179	16	j	j	PROPN
eurjchem-1783	180	1	=	=	SYM
eurjchem-1783	180	2	4	4	NUM
eurjchem-1783	180	3	hz	hz	NOUN
eurjchem-1783	180	4	,	,	PUNCT
eurjchem-1783	180	5	4h	4h	NOUN
eurjchem-1783	180	6	,	,	PUNCT
eurjchem-1783	180	7	piperazine	piperazine	NOUN
eurjchem-1783	180	8	-	-	PUNCT
eurjchem-1783	180	9	h	h	NOUN
eurjchem-1783	180	10	)	)	PUNCT
eurjchem-1783	180	11	,	,	PUNCT
eurjchem-1783	180	12	3.01	3.01	NUM
eurjchem-1783	180	13	(	(	PUNCT
eurjchem-1783	180	14	t	t	PROPN
eurjchem-1783	180	15	,	,	PUNCT
eurjchem-1783	180	16	j	j	PROPN
eurjchem-1783	181	1	=	=	SYM
eurjchem-1783	181	2	5	5	NUM
eurjchem-1783	181	3	hz	hz	VERB
eurjchem-1783	181	4	,	,	PUNCT
eurjchem-1783	181	5	4h	4h	NOUN
eurjchem-1783	181	6	,	,	PUNCT
eurjchem-1783	181	7	piperazine	piperazine	NOUN
eurjchem-1783	181	8	-	-	PUNCT
eurjchem-1783	181	9	h	h	NOUN
eurjchem-1783	181	10	)	)	PUNCT
eurjchem-1783	181	11	.	.	PUNCT
eurjchem-1783	182	1	13c	13c	NOUN
eurjchem-1783	182	2	nmr	nmr	NOUN
eurjchem-1783	182	3	(	(	PUNCT
eurjchem-1783	182	4	100	100	NUM
eurjchem-1783	182	5	mhz	mhz	NOUN
eurjchem-1783	182	6	,	,	PUNCT
eurjchem-1783	182	7	cdcl3	cdcl3	PROPN
eurjchem-1783	182	8	,	,	PUNCT
eurjchem-1783	182	9	δ	δ	PROPN
eurjchem-1783	182	10	,	,	PUNCT
eurjchem-1783	182	11	ppm	ppm	NUM
eurjchem-1783	182	12	):	):	PUNCT
eurjchem-1783	182	13	155.1	155.1	NUM
eurjchem-1783	182	14	(	(	PUNCT
eurjchem-1783	182	15	1c	1c	NOUN
eurjchem-1783	182	16	,	,	PUNCT
eurjchem-1783	182	17	ar	ar	NOUN
eurjchem-1783	182	18	-	-	NOUN
eurjchem-1783	182	19	c	c	NOUN
eurjchem-1783	182	20	)	)	PUNCT
eurjchem-1783	182	21	,	,	PUNCT
eurjchem-1783	182	22	142.2	142.2	NUM
eurjchem-1783	182	23	(	(	PUNCT
eurjchem-1783	182	24	1c	1c	NOUN
eurjchem-1783	182	25	,	,	PUNCT
eurjchem-1783	182	26	arc	arc	NOUN
eurjchem-1783	182	27	)	)	PUNCT
eurjchem-1783	182	28	,	,	PUNCT
eurjchem-1783	182	29	127.7	127.7	NUM
eurjchem-1783	182	30	(	(	PUNCT
eurjchem-1783	182	31	1c	1c	NOUN
eurjchem-1783	182	32	,	,	PUNCT
eurjchem-1783	182	33	ar	ar	NOUN
eurjchem-1783	182	34	-	-	NOUN
eurjchem-1783	182	35	c	c	NOUN
eurjchem-1783	182	36	)	)	PUNCT
eurjchem-1783	182	37	,	,	PUNCT
eurjchem-1783	182	38	126.7	126.7	NUM
eurjchem-1783	182	39	(	(	PUNCT
eurjchem-1783	182	40	1c	1c	NOUN
eurjchem-1783	182	41	,	,	PUNCT
eurjchem-1783	182	42	ar	ar	NOUN
eurjchem-1783	182	43	-	-	NOUN
eurjchem-1783	182	44	c	c	NOUN
eurjchem-1783	182	45	)	)	PUNCT
eurjchem-1783	182	46	,	,	PUNCT
eurjchem-1783	182	47	123.4	123.4	NUM
eurjchem-1783	182	48	(	(	PUNCT
eurjchem-1783	182	49	1c	1c	NOUN
eurjchem-1783	182	50	,	,	PUNCT
eurjchem-1783	182	51	ar	ar	NOUN
eurjchem-1783	182	52	-	-	NOUN
eurjchem-1783	182	53	c	c	NOUN
eurjchem-1783	182	54	)	)	PUNCT
eurjchem-1783	182	55	,	,	PUNCT
eurjchem-1783	182	56	119.3	119.3	NUM
eurjchem-1783	182	57	(	(	PUNCT
eurjchem-1783	182	58	1c	1c	NOUN
eurjchem-1783	182	59	,	,	PUNCT
eurjchem-1783	182	60	ar	ar	NOUN
eurjchem-1783	182	61	-	-	NOUN
eurjchem-1783	182	62	c	c	NOUN
eurjchem-1783	182	63	)	)	PUNCT
eurjchem-1783	182	64	,	,	PUNCT
eurjchem-1783	182	65	45.82	45.82	NUM
eurjchem-1783	182	66	(	(	PUNCT
eurjchem-1783	182	67	2c	2c	NOUN
eurjchem-1783	182	68	,	,	PUNCT
eurjchem-1783	182	69	piperazine	piperazine	NOUN
eurjchem-1783	182	70	-	-	PUNCT
eurjchem-1783	182	71	c	c	NOUN
eurjchem-1783	182	72	)	)	PUNCT
eurjchem-1783	182	73	,	,	PUNCT
eurjchem-1783	182	74	51.81	51.81	NUM
eurjchem-1783	182	75	(	(	PUNCT
eurjchem-1783	182	76	2c	2c	NOUN
eurjchem-1783	182	77	,	,	PUNCT
eurjchem-1783	182	78	piperazine	piperazine	NOUN
eurjchem-1783	182	79	-	-	PUNCT
eurjchem-1783	182	80	c	c	NOUN
eurjchem-1783	182	81	)	)	PUNCT
eurjchem-1783	182	82	.	.	PUNCT
eurjchem-1783	183	1	ms	ms	NOUN
eurjchem-1783	183	2	(	(	PUNCT
eurjchem-1783	183	3	m	m	PROPN
eurjchem-1783	183	4	/	/	SYM
eurjchem-1783	183	5	z	z	NOUN
eurjchem-1783	183	6	):	):	PUNCT
eurjchem-1783	183	7	226.1	226.1	NUM
eurjchem-1783	183	8	(	(	PUNCT
eurjchem-1783	183	9	m+	m+	NUM
eurjchem-1783	183	10	)	)	PUNCT
eurjchem-1783	183	11	.	.	PUNCT
eurjchem-1783	184	1	anal	anal	PROPN
eurjchem-1783	184	2	.	.	PUNCT
eurjchem-1783	184	3	calcd	calcd	NOUN
eurjchem-1783	184	4	.	.	PUNCT
eurjchem-1783	185	1	for	for	SCONJ
eurjchem-1783	185	2	c10h12fn3o2	c10h12fn3o2	PROPN
eurjchem-1783	185	3	:	:	PUNCT
eurjchem-1783	185	4	c	c	X
eurjchem-1783	185	5	,	,	PUNCT
eurjchem-1783	185	6	53.33	53.33	NUM
eurjchem-1783	185	7	;	;	PUNCT
eurjchem-1783	185	8	h	h	NOUN
eurjchem-1783	185	9	,	,	PUNCT
eurjchem-1783	185	10	5.37	5.37	NUM
eurjchem-1783	185	11	;	;	PUNCT
eurjchem-1783	185	12	n	n	CCONJ
eurjchem-1783	185	13	,	,	PUNCT
eurjchem-1783	185	14	18.66	18.66	NUM
eurjchem-1783	185	15	.	.	PUNCT
eurjchem-1783	185	16	found	find	VERB
eurjchem-1783	185	17	:	:	PUNCT
eurjchem-1783	186	1	c	c	X
eurjchem-1783	186	2	,	,	PUNCT
eurjchem-1783	186	3	53.32	53.32	NUM
eurjchem-1783	186	4	;	;	PUNCT
eurjchem-1783	186	5	h	h	NOUN
eurjchem-1783	186	6	,	,	PUNCT
eurjchem-1783	186	7	5.25	5.25	NUM
eurjchem-1783	186	8	;	;	PUNCT
eurjchem-1783	186	9	n	n	CCONJ
eurjchem-1783	186	10	,	,	PUNCT
eurjchem-1783	186	11	18.61	18.61	NUM
eurjchem-1783	186	12	%	%	NOUN
eurjchem-1783	186	13	.	.	PUNCT
eurjchem-1783	187	1	2.2.7	2.2.7	X
eurjchem-1783	187	2	.	.	PUNCT
eurjchem-1783	188	1	synthesis	synthesis	NOUN
eurjchem-1783	188	2	of	of	ADP
eurjchem-1783	188	3	tert	tert	NOUN
eurjchem-1783	188	4	-	-	PUNCT
eurjchem-1783	188	5	butyl	butyl	NOUN
eurjchem-1783	188	6	4-(2	4-(2	PROPN
eurjchem-1783	188	7	-	-	PUNCT
eurjchem-1783	188	8	fluoro-4	fluoro-4	NOUN
eurjchem-1783	188	9	-	-	PUNCT
eurjchem-1783	188	10	nitrophenyl	nitrophenyl	NOUN
eurjchem-1783	188	11	)	)	PUNCT
eurjchem-1783	188	12	piperazine-1	piperazine-1	NOUN
eurjchem-1783	188	13	-	-	NOUN
eurjchem-1783	188	14	carboxylate	carboxylate	NOUN
eurjchem-1783	188	15	(	(	PUNCT
eurjchem-1783	188	16	7	7	NUM
eurjchem-1783	188	17	)	)	PUNCT
eurjchem-1783	188	18	1-(2	1-(2	PROPN
eurjchem-1783	188	19	-	-	PUNCT
eurjchem-1783	188	20	fluoro-4	fluoro-4	NOUN
eurjchem-1783	188	21	-	-	PUNCT
eurjchem-1783	188	22	nitrophenyl	nitrophenyl	NOUN
eurjchem-1783	188	23	)	)	PUNCT
eurjchem-1783	188	24	piperazine	piperazine	NOUN
eurjchem-1783	188	25	(	(	PUNCT
eurjchem-1783	188	26	25	25	NUM
eurjchem-1783	188	27	g	g	NOUN
eurjchem-1783	188	28	,	,	PUNCT
eurjchem-1783	188	29	0.111	0.111	NUM
eurjchem-1783	188	30	mol	mol	NOUN
eurjchem-1783	188	31	)	)	PUNCT
eurjchem-1783	188	32	was	be	AUX
eurjchem-1783	188	33	dissolved	dissolve	VERB
eurjchem-1783	188	34	in	in	ADP
eurjchem-1783	188	35	dichloromethane	dichloromethane	NOUN
eurjchem-1783	188	36	(	(	PUNCT
eurjchem-1783	188	37	250	250	NUM
eurjchem-1783	188	38	ml	ml	NOUN
eurjchem-1783	188	39	)	)	PUNCT
eurjchem-1783	188	40	,	,	PUNCT
eurjchem-1783	188	41	added	add	VERB
eurjchem-1783	188	42	triethyl	triethyl	PROPN
eurjchem-1783	188	43	amine	amine	PROPN
eurjchem-1783	188	44	(	(	PUNCT
eurjchem-1783	188	45	13.47	13.47	NUM
eurjchem-1783	188	46	g	g	NOUN
eurjchem-1783	188	47	,	,	PUNCT
eurjchem-1783	188	48	0.133	0.133	NUM
eurjchem-1783	188	49	mol	mol	NOUN
eurjchem-1783	188	50	)	)	PUNCT
eurjchem-1783	188	51	and	and	CCONJ
eurjchem-1783	188	52	the	the	DET
eurjchem-1783	188	53	reaction	reaction	NOUN
eurjchem-1783	188	54	mixture	mixture	NOUN
eurjchem-1783	188	55	is	be	AUX
eurjchem-1783	188	56	cooled	cool	VERB
eurjchem-1783	188	57	to	to	ADP
eurjchem-1783	188	58	-10	-10	PUNCT
eurjchem-1783	188	59	°	°	PRON
eurjchem-1783	188	60	c	c	NOUN
eurjchem-1783	188	61	.	.	PUNCT
eurjchem-1783	189	1	to	to	ADP
eurjchem-1783	189	2	this	this	DET
eurjchem-1783	189	3	di	di	NOUN
eurjchem-1783	189	4	-	-	PUNCT
eurjchem-1783	189	5	tert	tert	NOUN
eurjchem-1783	189	6	-	-	PUNCT
eurjchem-1783	189	7	butyldicarbonate	butyldicarbonate	NOUN
eurjchem-1783	189	8	(	(	PUNCT
eurjchem-1783	189	9	boc	boc	NOUN
eurjchem-1783	189	10	anhydride	anhydride	NOUN
eurjchem-1783	189	11	)	)	PUNCT
eurjchem-1783	189	12	(	(	PUNCT
eurjchem-1783	189	13	26.63	26.63	NUM
eurjchem-1783	189	14	g	g	NOUN
eurjchem-1783	189	15	,	,	PUNCT
eurjchem-1783	189	16	0.122	0.122	NUM
eurjchem-1783	189	17	mol	mol	NOUN
eurjchem-1783	189	18	)	)	PUNCT
eurjchem-1783	189	19	was	be	AUX
eurjchem-1783	189	20	added	add	VERB
eurjchem-1783	189	21	very	very	ADV
eurjchem-1783	189	22	slowly	slowly	ADV
eurjchem-1783	189	23	by	by	ADP
eurjchem-1783	189	24	keeping	keep	VERB
eurjchem-1783	189	25	temperature	temperature	NOUN
eurjchem-1783	189	26	between	between	ADP
eurjchem-1783	189	27	-10–0	-10–0	PROPN
eurjchem-1783	189	28	°	°	PROPN
eurjchem-1783	189	29	c	c	PROPN
eurjchem-1783	189	30	,	,	PUNCT
eurjchem-1783	189	31	after	after	SCONJ
eurjchem-1783	189	32	the	the	DET
eurjchem-1783	189	33	completion	completion	NOUN
eurjchem-1783	189	34	of	of	ADP
eurjchem-1783	189	35	addition	addition	NOUN
eurjchem-1783	189	36	of	of	ADP
eurjchem-1783	189	37	boc	boc	NOUN
eurjchem-1783	189	38	anhydride	anhydride	NOUN
eurjchem-1783	189	39	reaction	reaction	NOUN
eurjchem-1783	189	40	was	be	AUX
eurjchem-1783	189	41	warmed	warm	VERB
eurjchem-1783	189	42	to	to	ADP
eurjchem-1783	189	43	room	room	NOUN
eurjchem-1783	189	44	temperature	temperature	NOUN
eurjchem-1783	189	45	and	and	CCONJ
eurjchem-1783	189	46	a	a	DET
eurjchem-1783	189	47	stirred	stir	VERB
eurjchem-1783	189	48	at	at	ADP
eurjchem-1783	189	49	the	the	DET
eurjchem-1783	189	50	same	same	ADJ
eurjchem-1783	189	51	for	for	ADP
eurjchem-1783	189	52	2	2	NUM
eurjchem-1783	189	53	hr	hr	NOUN
eurjchem-1783	189	54	.	.	PUNCT
eurjchem-1783	190	1	added	add	VERB
eurjchem-1783	190	2	water	water	NOUN
eurjchem-1783	190	3	(	(	PUNCT
eurjchem-1783	190	4	100	100	NUM
eurjchem-1783	190	5	ml	ml	NOUN
eurjchem-1783	190	6	)	)	PUNCT
eurjchem-1783	190	7	,	,	PUNCT
eurjchem-1783	190	8	organic	organic	ADJ
eurjchem-1783	190	9	layer	layer	NOUN
eurjchem-1783	190	10	was	be	AUX
eurjchem-1783	190	11	separated	separate	VERB
eurjchem-1783	190	12	,	,	PUNCT
eurjchem-1783	190	13	aqueous	aqueous	ADJ
eurjchem-1783	190	14	layer	layer	NOUN
eurjchem-1783	190	15	was	be	AUX
eurjchem-1783	190	16	extracted	extract	VERB
eurjchem-1783	190	17	with	with	ADP
eurjchem-1783	190	18	dichloromethane(75	dichloromethane(75	NOUN
eurjchem-1783	190	19	ml	ml	VERB
eurjchem-1783	190	20	×	×	NOUN
eurjchem-1783	190	21	3	3	NUM
eurjchem-1783	190	22	)	)	PUNCT
eurjchem-1783	190	23	and	and	CCONJ
eurjchem-1783	190	24	the	the	DET
eurjchem-1783	190	25	combined	combine	VERB
eurjchem-1783	190	26	organic	organic	ADJ
eurjchem-1783	190	27	layer	layer	NOUN
eurjchem-1783	190	28	was	be	AUX
eurjchem-1783	190	29	washed(100	washed(100	PROPN
eurjchem-1783	190	30	ml	ml	PROPN
eurjchem-1783	190	31	×	×	PROPN
eurjchem-1783	190	32	2	2	NUM
eurjchem-1783	190	33	)	)	PUNCT
eurjchem-1783	190	34	with	with	ADP
eurjchem-1783	190	35	water	water	NOUN
eurjchem-1783	190	36	(	(	PUNCT
eurjchem-1783	190	37	100	100	NUM
eurjchem-1783	190	38	ml	ml	NOUN
eurjchem-1783	190	39	×	×	PROPN
eurjchem-1783	190	40	2	2	NUM
eurjchem-1783	190	41	)	)	PUNCT
eurjchem-1783	190	42	,	,	PUNCT
eurjchem-1783	190	43	brine	brine	NOUN
eurjchem-1783	190	44	(	(	PUNCT
eurjchem-1783	190	45	100	100	NUM
eurjchem-1783	190	46	ml	ml	PART
eurjchem-1783	190	47	×	×	PROPN
eurjchem-1783	190	48	1	1	NUM
eurjchem-1783	190	49	)	)	PUNCT
eurjchem-1783	190	50	,	,	PUNCT
eurjchem-1783	190	51	dried	dry	VERB
eurjchem-1783	190	52	over	over	ADP
eurjchem-1783	190	53	na2so4	na2so4	NOUN
eurjchem-1783	190	54	,	,	PUNCT
eurjchem-1783	190	55	filtered	filter	VERB
eurjchem-1783	190	56	and	and	CCONJ
eurjchem-1783	190	57	concentrated	concentrate	VERB
eurjchem-1783	190	58	to	to	PART
eurjchem-1783	190	59	get	get	VERB
eurjchem-1783	190	60	the	the	DET
eurjchem-1783	190	61	crude	crude	ADJ
eurjchem-1783	190	62	mass	mass	NOUN
eurjchem-1783	190	63	,	,	PUNCT
eurjchem-1783	190	64	which	which	PRON
eurjchem-1783	190	65	was	be	AUX
eurjchem-1783	190	66	further	far	ADV
eurjchem-1783	190	67	purified	purify	VERB
eurjchem-1783	190	68	by	by	ADP
eurjchem-1783	190	69	flash	flash	NOUN
eurjchem-1783	190	70	column	column	NOUN
eurjchem-1783	190	71	chromatography	chromatography	NOUN
eurjchem-1783	190	72	using	use	VERB
eurjchem-1783	190	73	hexane	hexane	NOUN
eurjchem-1783	190	74	and	and	CCONJ
eurjchem-1783	190	75	ethyl	ethyl	PROPN
eurjchem-1783	190	76	acetate	acetate	PROPN
eurjchem-1783	190	77	to	to	PART
eurjchem-1783	190	78	give	give	VERB
eurjchem-1783	190	79	a	a	DET
eurjchem-1783	190	80	pure	pure	ADJ
eurjchem-1783	190	81	product	product	NOUN
eurjchem-1783	190	82	as	as	ADP
eurjchem-1783	190	83	pale	pale	ADJ
eurjchem-1783	190	84	yellow	yellow	ADJ
eurjchem-1783	190	85	solid	solid	ADJ
eurjchem-1783	190	86	(	(	PUNCT
eurjchem-1783	190	87	scheme	scheme	NOUN
eurjchem-1783	190	88	3	3	NUM
eurjchem-1783	190	89	)	)	PUNCT
eurjchem-1783	190	90	.	.	PUNCT
eurjchem-1783	191	1	color	color	NOUN
eurjchem-1783	191	2	:	:	PUNCT
eurjchem-1783	191	3	pale	pale	ADJ
eurjchem-1783	191	4	yellow	yellow	ADJ
eurjchem-1783	191	5	.	.	PUNCT
eurjchem-1783	192	1	yield	yield	NOUN
eurjchem-1783	192	2	:	:	PUNCT
eurjchem-1783	192	3	98	98	NUM
eurjchem-1783	192	4	%	%	NOUN
eurjchem-1783	192	5	.	.	PUNCT
eurjchem-1783	193	1	m.p	m.p	PROPN
eurjchem-1783	193	2	.	.	PROPN
eurjchem-1783	193	3	:	:	PUNCT
eurjchem-1783	194	1	121	121	NUM
eurjchem-1783	194	2	-	-	SYM
eurjchem-1783	194	3	122	122	NUM
eurjchem-1783	194	4	°	°	SYM
eurjchem-1783	194	5	c	c	NOUN
eurjchem-1783	194	6	.	.	PUNCT
eurjchem-1783	195	1	1h	1h	NUM
eurjchem-1783	195	2	nmr	nmr	NOUN
eurjchem-1783	195	3	(	(	PUNCT
eurjchem-1783	195	4	400	400	NUM
eurjchem-1783	195	5	mhz	mhz	NOUN
eurjchem-1783	195	6	,	,	PUNCT
eurjchem-1783	195	7	cdcl3	cdcl3	PROPN
eurjchem-1783	195	8	,	,	PUNCT
eurjchem-1783	195	9	δ	δ	PROPN
eurjchem-1783	195	10	,	,	PUNCT
eurjchem-1783	195	11	ppm	ppm	NUM
eurjchem-1783	195	12	):	):	PUNCT
eurjchem-1783	195	13	8.01	8.01	NUM
eurjchem-1783	195	14	-	-	SYM
eurjchem-1783	195	15	7.98	7.98	NUM
eurjchem-1783	195	16	(	(	PUNCT
eurjchem-1783	195	17	dd	dd	NOUN
eurjchem-1783	195	18	,	,	PUNCT
eurjchem-1783	195	19	j	j	PROPN
eurjchem-1783	196	1	=	=	SYM
eurjchem-1783	196	2	2.25	2.25	NUM
eurjchem-1783	196	3	hz	hz	NOUN
eurjchem-1783	196	4	,	,	PUNCT
eurjchem-1783	196	5	1h	1h	NUM
eurjchem-1783	196	6	,	,	PUNCT
eurjchem-1783	196	7	ar	ar	NOUN
eurjchem-1783	196	8	-	-	NOUN
eurjchem-1783	196	9	h	h	NOUN
eurjchem-1783	196	10	)	)	PUNCT
eurjchem-1783	196	11	,	,	PUNCT
eurjchem-1783	196	12	7.90	7.90	NUM
eurjchem-1783	196	13	(	(	PUNCT
eurjchem-1783	196	14	dd	dd	PROPN
eurjchem-1783	196	15	,	,	PUNCT
eurjchem-1783	196	16	j	j	PROPN
eurjchem-1783	197	1	=	=	SYM
eurjchem-1783	197	2	12.92	12.92	NUM
eurjchem-1783	197	3	hz	hz	NOUN
eurjchem-1783	197	4	,	,	PUNCT
eurjchem-1783	197	5	1h	1h	NUM
eurjchem-1783	197	6	,	,	PUNCT
eurjchem-1783	197	7	ar	ar	NOUN
eurjchem-1783	197	8	-	-	NOUN
eurjchem-1783	197	9	h	h	NOUN
eurjchem-1783	197	10	)	)	PUNCT
eurjchem-1783	197	11	6.94	6.94	NUM
eurjchem-1783	197	12	(	(	PUNCT
eurjchem-1783	197	13	t	t	PROPN
eurjchem-1783	197	14	,	,	PUNCT
eurjchem-1783	197	15	j	j	PROPN
eurjchem-1783	198	1	=	=	PROPN
eurjchem-1783	198	2	8.72	8.72	NUM
eurjchem-1783	198	3	hz	hz	NOUN
eurjchem-1783	198	4	,	,	PUNCT
eurjchem-1783	198	5	1h	1h	NUM
eurjchem-1783	198	6	,	,	PUNCT
eurjchem-1783	198	7	ar	ar	NOUN
eurjchem-1783	198	8	-	-	NOUN
eurjchem-1783	198	9	h	h	NOUN
eurjchem-1783	198	10	)	)	PUNCT
eurjchem-1783	198	11	,	,	PUNCT
eurjchem-1783	198	12	3.61	3.61	NUM
eurjchem-1783	198	13	(	(	PUNCT
eurjchem-1783	198	14	t	t	PROPN
eurjchem-1783	198	15	,	,	PUNCT
eurjchem-1783	198	16	j	j	PROPN
eurjchem-1783	198	17	=	=	SYM
eurjchem-1783	198	18	4.84	4.84	NUM
eurjchem-1783	198	19	hz	hz	NOUN
eurjchem-1783	198	20	,	,	PUNCT
eurjchem-1783	198	21	4h	4h	NOUN
eurjchem-1783	198	22	,	,	PUNCT
eurjchem-1783	198	23	piperazine	piperazine	NOUN
eurjchem-1783	198	24	-	-	PUNCT
eurjchem-1783	198	25	h	h	NOUN
eurjchem-1783	198	26	)	)	PUNCT
eurjchem-1783	198	27	,	,	PUNCT
eurjchem-1783	198	28	3.24	3.24	NUM
eurjchem-1783	198	29	(	(	PUNCT
eurjchem-1783	198	30	t	t	PROPN
eurjchem-1783	198	31	,	,	PUNCT
eurjchem-1783	198	32	j	j	PROPN
eurjchem-1783	199	1	=	=	SYM
eurjchem-1783	199	2	5.08	5.08	NUM
eurjchem-1783	199	3	hz	hz	NOUN
eurjchem-1783	199	4	,	,	PUNCT
eurjchem-1783	199	5	4h	4h	NUM
eurjchem-1783	199	6	,	,	PUNCT
eurjchem-1783	199	7	piperazineh	piperazineh	PROPN
eurjchem-1783	199	8	)	)	PUNCT
eurjchem-1783	199	9	,	,	PUNCT
eurjchem-1783	199	10	1.49	1.49	NUM
eurjchem-1783	199	11	(	(	PUNCT
eurjchem-1783	199	12	s	s	PROPN
eurjchem-1783	199	13	,	,	PUNCT
eurjchem-1783	199	14	9h	9h	NUM
eurjchem-1783	199	15	,	,	PUNCT
eurjchem-1783	199	16	boc	boc	NOUN
eurjchem-1783	199	17	-	-	NOUN
eurjchem-1783	199	18	h	h	NOUN
eurjchem-1783	199	19	)	)	PUNCT
eurjchem-1783	199	20	.	.	PUNCT
eurjchem-1783	200	1	13c	13c	NOUN
eurjchem-1783	200	2	nmr	nmr	NOUN
eurjchem-1783	200	3	(	(	PUNCT
eurjchem-1783	200	4	100	100	NUM
eurjchem-1783	200	5	mhz	mhz	NOUN
eurjchem-1783	200	6	,	,	PUNCT
eurjchem-1783	200	7	cdcl3	cdcl3	PROPN
eurjchem-1783	200	8	,	,	PUNCT
eurjchem-1783	200	9	δ	δ	PROPN
eurjchem-1783	200	10	,	,	PUNCT
eurjchem-1783	200	11	ppm	ppm	NUM
eurjchem-1783	200	12	):	):	PUNCT
eurjchem-1783	200	13	154.6	154.6	NUM
eurjchem-1783	200	14	(	(	PUNCT
eurjchem-1783	200	15	1c	1c	NOUN
eurjchem-1783	200	16	,	,	PUNCT
eurjchem-1783	200	17	co	co	NOUN
eurjchem-1783	200	18	)	)	PUNCT
eurjchem-1783	200	19	,	,	PUNCT
eurjchem-1783	200	20	153.7	153.7	NUM
eurjchem-1783	200	21	(	(	PUNCT
eurjchem-1783	200	22	1c	1c	NOUN
eurjchem-1783	200	23	,	,	PUNCT
eurjchem-1783	200	24	ar	ar	NOUN
eurjchem-1783	200	25	-	-	NOUN
eurjchem-1783	200	26	c	c	NOUN
eurjchem-1783	200	27	)	)	PUNCT
eurjchem-1783	200	28	,	,	PUNCT
eurjchem-1783	200	29	142.6	142.6	NUM
eurjchem-1783	200	30	(	(	PUNCT
eurjchem-1783	200	31	1c	1c	NOUN
eurjchem-1783	200	32	,	,	PUNCT
eurjchem-1783	200	33	ar	ar	NOUN
eurjchem-1783	200	34	-	-	NOUN
eurjchem-1783	200	35	c	c	NOUN
eurjchem-1783	200	36	)	)	PUNCT
eurjchem-1783	200	37	,	,	PUNCT
eurjchem-1783	200	38	128	128	NUM
eurjchem-1783	200	39	(	(	PUNCT
eurjchem-1783	200	40	1c	1c	NOUN
eurjchem-1783	200	41	,	,	PUNCT
eurjchem-1783	200	42	arc	arc	NOUN
eurjchem-1783	200	43	)	)	PUNCT
eurjchem-1783	200	44	,	,	PUNCT
eurjchem-1783	200	45	126.7	126.7	NUM
eurjchem-1783	200	46	(	(	PUNCT
eurjchem-1783	200	47	1c	1c	NOUN
eurjchem-1783	200	48	,	,	PUNCT
eurjchem-1783	200	49	ar	ar	NOUN
eurjchem-1783	200	50	-	-	NOUN
eurjchem-1783	200	51	c	c	NOUN
eurjchem-1783	200	52	)	)	PUNCT
eurjchem-1783	200	53	,	,	PUNCT
eurjchem-1783	200	54	123.4	123.4	NUM
eurjchem-1783	200	55	(	(	PUNCT
eurjchem-1783	200	56	1c	1c	NOUN
eurjchem-1783	200	57	,	,	PUNCT
eurjchem-1783	200	58	ar	ar	NOUN
eurjchem-1783	200	59	-	-	NOUN
eurjchem-1783	200	60	c	c	NOUN
eurjchem-1783	200	61	)	)	PUNCT
eurjchem-1783	200	62	,	,	PUNCT
eurjchem-1783	200	63	119.5	119.5	NUM
eurjchem-1783	200	64	(	(	PUNCT
eurjchem-1783	200	65	1c	1c	NOUN
eurjchem-1783	200	66	,	,	PUNCT
eurjchem-1783	200	67	ar	ar	NOUN
eurjchem-1783	200	68	-	-	NOUN
eurjchem-1783	200	69	c	c	NOUN
eurjchem-1783	200	70	)	)	PUNCT
eurjchem-1783	200	71	,	,	PUNCT
eurjchem-1783	200	72	80	80	NUM
eurjchem-1783	200	73	(	(	PUNCT
eurjchem-1783	200	74	1c	1c	NOUN
eurjchem-1783	200	75	,	,	PUNCT
eurjchem-1783	200	76	c	c	NOUN
eurjchem-1783	200	77	-	-	PUNCT
eurjchem-1783	200	78	ch3	ch3	NOUN
eurjchem-1783	200	79	)	)	PUNCT
eurjchem-1783	200	80	,	,	PUNCT
eurjchem-1783	200	81	50.1	50.1	NUM
eurjchem-1783	200	82	(	(	PUNCT
eurjchem-1783	200	83	2c	2c	NOUN
eurjchem-1783	200	84	,	,	PUNCT
eurjchem-1783	200	85	piperazine	piperazine	NOUN
eurjchem-1783	200	86	-	-	PUNCT
eurjchem-1783	200	87	c	c	NOUN
eurjchem-1783	200	88	)	)	PUNCT
eurjchem-1783	200	89	,	,	PUNCT
eurjchem-1783	200	90	50.1	50.1	NUM
eurjchem-1783	200	91	(	(	PUNCT
eurjchem-1783	200	92	2c	2c	NOUN
eurjchem-1783	200	93	,	,	PUNCT
eurjchem-1783	200	94	piperazine	piperazine	NOUN
eurjchem-1783	200	95	-	-	PUNCT
eurjchem-1783	200	96	c	c	NOUN
eurjchem-1783	200	97	)	)	PUNCT
eurjchem-1783	200	98	,	,	PUNCT
eurjchem-1783	200	99	28.5	28.5	NUM
eurjchem-1783	200	100	(	(	PUNCT
eurjchem-1783	200	101	3c	3c	NUM
eurjchem-1783	200	102	,	,	PUNCT
eurjchem-1783	200	103	ch3	ch3	PROPN
eurjchem-1783	200	104	)	)	PUNCT
eurjchem-1783	200	105	.	.	PUNCT
eurjchem-1783	201	1	ms	ms	NOUN
eurjchem-1783	201	2	(	(	PUNCT
eurjchem-1783	201	3	m	m	PROPN
eurjchem-1783	201	4	/	/	SYM
eurjchem-1783	201	5	z	z	NOUN
eurjchem-1783	201	6	):	):	PUNCT
eurjchem-1783	201	7	326	326	NUM
eurjchem-1783	201	8	(	(	PUNCT
eurjchem-1783	201	9	m+	m+	NUM
eurjchem-1783	201	10	)	)	PUNCT
eurjchem-1783	201	11	.	.	PUNCT
eurjchem-1783	202	1	anal	anal	PROPN
eurjchem-1783	202	2	.	.	PUNCT
eurjchem-1783	202	3	calcd	calcd	NOUN
eurjchem-1783	202	4	.	.	PUNCT
eurjchem-1783	203	1	for	for	SCONJ
eurjchem-1783	203	2	c15h20fn3o4	c15h20fn3o4	PROPN
eurjchem-1783	203	3	:	:	PUNCT
eurjchem-1783	203	4	c	c	X
eurjchem-1783	203	5	,	,	PUNCT
eurjchem-1783	203	6	55.38	55.38	NUM
eurjchem-1783	203	7	;	;	PUNCT
eurjchem-1783	203	8	h	h	NOUN
eurjchem-1783	203	9	,	,	PUNCT
eurjchem-1783	203	10	6.20	6.20	NUM
eurjchem-1783	203	11	;	;	PUNCT
eurjchem-1783	203	12	n	n	CCONJ
eurjchem-1783	203	13	,	,	PUNCT
eurjchem-1783	203	14	12.92	12.92	NUM
eurjchem-1783	203	15	.	.	PUNCT
eurjchem-1783	203	16	found	find	VERB
eurjchem-1783	203	17	:	:	PUNCT
eurjchem-1783	204	1	c	c	X
eurjchem-1783	204	2	,	,	PUNCT
eurjchem-1783	204	3	55.41	55.41	NUM
eurjchem-1783	204	4	;	;	PUNCT
eurjchem-1783	205	1	h	h	NOUN
eurjchem-1783	205	2	,	,	PUNCT
eurjchem-1783	205	3	6.15	6.15	NUM
eurjchem-1783	205	4	;	;	PUNCT
eurjchem-1783	205	5	n	n	CCONJ
eurjchem-1783	205	6	,	,	PUNCT
eurjchem-1783	205	7	12.82	12.82	NUM
eurjchem-1783	205	8	%	%	NOUN
eurjchem-1783	205	9	.	.	PUNCT
eurjchem-1783	206	1	2.2.8	2.2.8	X
eurjchem-1783	206	2	.	.	PUNCT
eurjchem-1783	207	1	synthesis	synthesis	NOUN
eurjchem-1783	207	2	of	of	ADP
eurjchem-1783	207	3	tert	tert	NOUN
eurjchem-1783	207	4	-	-	PUNCT
eurjchem-1783	207	5	butyl	butyl	NOUN
eurjchem-1783	207	6	4-(4	4-(4	PROPN
eurjchem-1783	207	7	-	-	PUNCT
eurjchem-1783	207	8	amino-2	amino-2	VERB
eurjchem-1783	207	9	-	-	PUNCT
eurjchem-1783	207	10	fluorophenyl	fluorophenyl	NOUN
eurjchem-1783	207	11	)	)	PUNCT
eurjchem-1783	207	12	piperazine-1	piperazine-1	NOUN
eurjchem-1783	207	13	-	-	NOUN
eurjchem-1783	207	14	carboxylate	carboxylate	NOUN
eurjchem-1783	207	15	(	(	PUNCT
eurjchem-1783	207	16	8)	8)	NUM
eurjchem-1783	207	17	tert	tert	NOUN
eurjchem-1783	207	18	-	-	PUNCT
eurjchem-1783	207	19	butyl	butyl	NOUN
eurjchem-1783	207	20	4-(2	4-(2	PROPN
eurjchem-1783	207	21	-	-	PUNCT
eurjchem-1783	207	22	fluoro-4	fluoro-4	NOUN
eurjchem-1783	207	23	-	-	PUNCT
eurjchem-1783	207	24	nitrophenyl)piperazine-1	nitrophenyl)piperazine-1	NOUN
eurjchem-1783	207	25	-	-	PUNCT
eurjchem-1783	207	26	carboxylate	carboxylate	NOUN
eurjchem-1783	207	27	(	(	PUNCT
eurjchem-1783	207	28	30	30	NUM
eurjchem-1783	207	29	g	g	NOUN
eurjchem-1783	207	30	,	,	PUNCT
eurjchem-1783	207	31	0.092	0.092	NUM
eurjchem-1783	207	32	mol	mol	NOUN
eurjchem-1783	207	33	)	)	PUNCT
eurjchem-1783	207	34	was	be	AUX
eurjchem-1783	207	35	dissolved	dissolve	VERB
eurjchem-1783	207	36	in	in	ADP
eurjchem-1783	207	37	ethanol	ethanol	NOUN
eurjchem-1783	207	38	(	(	PUNCT
eurjchem-1783	207	39	250	250	NUM
eurjchem-1783	207	40	ml	ml	NOUN
eurjchem-1783	207	41	)	)	PUNCT
eurjchem-1783	207	42	in	in	ADP
eurjchem-1783	207	43	a	a	DET
eurjchem-1783	207	44	three	three	NUM
eurjchem-1783	207	45	necked	neck	VERB
eurjchem-1783	207	46	round	round	ADJ
eurjchem-1783	207	47	bottom	bottom	ADJ
eurjchem-1783	207	48	flask	flask	NOUN
eurjchem-1783	207	49	fitted	fit	VERB
eurjchem-1783	207	50	with	with	ADP
eurjchem-1783	207	51	the	the	DET
eurjchem-1783	207	52	condenser	condenser	NOUN
eurjchem-1783	207	53	and	and	CCONJ
eurjchem-1783	207	54	cooled	cool	VERB
eurjchem-1783	207	55	to	to	ADP
eurjchem-1783	207	56	-10	-10	PUNCT
eurjchem-1783	207	57	°	°	PRON
eurjchem-1783	207	58	c	c	NOUN
eurjchem-1783	207	59	.	.	PUNCT
eurjchem-1783	208	1	raney	raney	PROPN
eurjchem-1783	208	2	nicked	nick	VERB
eurjchem-1783	208	3	(	(	PUNCT
eurjchem-1783	208	4	1.5	1.5	NUM
eurjchem-1783	208	5	g	g	NOUN
eurjchem-1783	208	6	)	)	PUNCT
eurjchem-1783	208	7	was	be	AUX
eurjchem-1783	208	8	suspended	suspend	VERB
eurjchem-1783	208	9	in	in	ADP
eurjchem-1783	208	10	ethanol	ethanol	NOUN
eurjchem-1783	208	11	(	(	PUNCT
eurjchem-1783	208	12	50	50	NUM
eurjchem-1783	208	13	ml	ml	NOUN
eurjchem-1783	208	14	)	)	PUNCT
eurjchem-1783	208	15	was	be	AUX
eurjchem-1783	208	16	introduced	introduce	VERB
eurjchem-1783	208	17	in	in	ADP
eurjchem-1783	208	18	to	to	ADP
eurjchem-1783	208	19	the	the	DET
eurjchem-1783	208	20	flask	flask	NOUN
eurjchem-1783	208	21	at	at	ADP
eurjchem-1783	208	22	-10	-10	PUNCT
eurjchem-1783	208	23	°	°	PRON
eurjchem-1783	208	24	c	c	NOUN
eurjchem-1783	208	25	.	.	PUNCT
eurjchem-1783	208	26	hydrazine	hydrazine	NOUN
eurjchem-1783	208	27	hydrate	hydrate	NOUN
eurjchem-1783	208	28	(	(	PUNCT
eurjchem-1783	208	29	5.73	5.73	NUM
eurjchem-1783	208	30	ml	ml	NOUN
eurjchem-1783	208	31	,	,	PUNCT
eurjchem-1783	208	32	0.184	0.184	NUM
eurjchem-1783	208	33	mol	mol	NOUN
eurjchem-1783	208	34	)	)	PUNCT
eurjchem-1783	208	35	was	be	AUX
eurjchem-1783	208	36	added	add	VERB
eurjchem-1783	208	37	to	to	ADP
eurjchem-1783	208	38	the	the	DET
eurjchem-1783	208	39	flask	flask	NOUN
eurjchem-1783	208	40	through	through	ADP
eurjchem-1783	208	41	the	the	DET
eurjchem-1783	208	42	syringe	syringe	NOUN
eurjchem-1783	208	43	by	by	ADP
eurjchem-1783	208	44	maintaining	maintain	VERB
eurjchem-1783	208	45	the	the	DET
eurjchem-1783	208	46	temperature	temperature	NOUN
eurjchem-1783	208	47	below	below	ADP
eurjchem-1783	208	48	0	0	NUM
eurjchem-1783	209	1	°	°	ADP
eurjchem-1783	209	2	c	c	NOUN
eurjchem-1783	209	3	.	.	PUNCT
eurjchem-1783	210	1	reaction	reaction	NOUN
eurjchem-1783	210	2	was	be	AUX
eurjchem-1783	210	3	stirred	stir	VERB
eurjchem-1783	210	4	at	at	ADP
eurjchem-1783	210	5	room	room	NOUN
eurjchem-1783	210	6	temperature	temperature	NOUN
eurjchem-1783	210	7	for	for	ADP
eurjchem-1783	210	8	30	30	NUM
eurjchem-1783	210	9	mins	min	NOUN
eurjchem-1783	210	10	and	and	CCONJ
eurjchem-1783	210	11	2018	2018	NUM
eurjchem-1783	210	12	–	–	PUNCT
eurjchem-1783	210	13	european	european	ADJ
eurjchem-1783	210	14	journal	journal	NOUN
eurjchem-1783	210	15	of	of	ADP
eurjchem-1783	210	16	chemistry	chemistry	NOUN
eurjchem-1783	210	17	–	–	PUNCT
eurjchem-1783	210	18	cc	cc	NOUN
eurjchem-1783	210	19	by	by	ADP
eurjchem-1783	210	20	nc	nc	PROPN
eurjchem-1783	210	21	–	–	PUNCT
eurjchem-1783	210	22	doi	doi	PROPN
eurjchem-1783	210	23	:	:	PUNCT
eurjchem-1783	210	24	10.5155	10.5155	NUM
eurjchem-1783	210	25	/	/	SYM
eurjchem-1783	210	26	eurjchem.9.4.353	eurjchem.9.4.353	PROPN
eurjchem-1783	210	27	-	-	SYM
eurjchem-1783	210	28	359.1783	359.1783	NUM
eurjchem-1783	210	29	siddaraj	siddaraj	ADJ
eurjchem-1783	210	30	et	et	NOUN
eurjchem-1783	210	31	al	al	PROPN
eurjchem-1783	210	32	.	.	PUNCT
eurjchem-1783	210	33	/	/	SYM
eurjchem-1783	210	34	european	european	PROPN
eurjchem-1783	210	35	journal	journal	PROPN
eurjchem-1783	210	36	of	of	ADP
eurjchem-1783	210	37	chemistry	chemistry	NOUN
eurjchem-1783	210	38	9	9	NUM
eurjchem-1783	210	39	(	(	PUNCT
eurjchem-1783	210	40	4	4	NUM
eurjchem-1783	210	41	)	)	PUNCT
eurjchem-1783	210	42	(	(	PUNCT
eurjchem-1783	210	43	2018	2018	NUM
eurjchem-1783	210	44	)	)	PUNCT
eurjchem-1783	210	45	353	353	NUM
eurjchem-1783	210	46	-	-	SYM
eurjchem-1783	210	47	359	359	NUM
eurjchem-1783	210	48	357	357	NUM
eurjchem-1783	210	49	the	the	DET
eurjchem-1783	210	50	completion	completion	NOUN
eurjchem-1783	210	51	of	of	ADP
eurjchem-1783	210	52	the	the	DET
eurjchem-1783	210	53	reaction	reaction	NOUN
eurjchem-1783	210	54	was	be	AUX
eurjchem-1783	210	55	monitored	monitor	VERB
eurjchem-1783	210	56	by	by	ADP
eurjchem-1783	210	57	tlc	tlc	PROPN
eurjchem-1783	210	58	.	.	PUNCT
eurjchem-1783	211	1	after	after	ADP
eurjchem-1783	211	2	the	the	DET
eurjchem-1783	211	3	completion	completion	NOUN
eurjchem-1783	211	4	the	the	DET
eurjchem-1783	211	5	reaction	reaction	NOUN
eurjchem-1783	211	6	mass	mass	NOUN
eurjchem-1783	211	7	was	be	AUX
eurjchem-1783	211	8	filtered	filter	VERB
eurjchem-1783	211	9	through	through	ADP
eurjchem-1783	211	10	the	the	DET
eurjchem-1783	211	11	celite	celite	ADJ
eurjchem-1783	211	12	bed	bed	NOUN
eurjchem-1783	211	13	to	to	PART
eurjchem-1783	211	14	remove	remove	VERB
eurjchem-1783	211	15	raney	raney	NOUN
eurjchem-1783	211	16	nickel	nickel	NOUN
eurjchem-1783	211	17	,	,	PUNCT
eurjchem-1783	211	18	washed	wash	VERB
eurjchem-1783	211	19	with	with	ADP
eurjchem-1783	211	20	ethanol	ethanol	NOUN
eurjchem-1783	211	21	(	(	PUNCT
eurjchem-1783	211	22	2×50	2×50	NUM
eurjchem-1783	211	23	ml	ml	NOUN
eurjchem-1783	211	24	)	)	PUNCT
eurjchem-1783	211	25	,	,	PUNCT
eurjchem-1783	211	26	concentrated	concentrate	VERB
eurjchem-1783	211	27	to	to	PART
eurjchem-1783	211	28	give	give	VERB
eurjchem-1783	211	29	crude	crude	ADJ
eurjchem-1783	211	30	product	product	NOUN
eurjchem-1783	211	31	.	.	PUNCT
eurjchem-1783	212	1	it	it	PRON
eurjchem-1783	212	2	was	be	AUX
eurjchem-1783	212	3	added	add	VERB
eurjchem-1783	212	4	diethyl	diethyl	NOUN
eurjchem-1783	212	5	ether	ether	NOUN
eurjchem-1783	212	6	(	(	PUNCT
eurjchem-1783	212	7	3×100	3×100	NUM
eurjchem-1783	212	8	ml	ml	NOUN
eurjchem-1783	212	9	)	)	PUNCT
eurjchem-1783	212	10	and	and	CCONJ
eurjchem-1783	212	11	stirred	stir	VERB
eurjchem-1783	212	12	for	for	ADP
eurjchem-1783	212	13	15	15	NUM
eurjchem-1783	212	14	mins	min	NOUN
eurjchem-1783	212	15	,	,	PUNCT
eurjchem-1783	212	16	filtered	filter	VERB
eurjchem-1783	212	17	and	and	CCONJ
eurjchem-1783	212	18	dried	dry	VERB
eurjchem-1783	212	19	to	to	PART
eurjchem-1783	212	20	give	give	VERB
eurjchem-1783	212	21	pure	pure	ADJ
eurjchem-1783	212	22	product	product	NOUN
eurjchem-1783	212	23	as	as	ADP
eurjchem-1783	212	24	light	light	ADJ
eurjchem-1783	212	25	brown	brown	ADJ
eurjchem-1783	212	26	solid	solid	ADJ
eurjchem-1783	212	27	(	(	PUNCT
eurjchem-1783	212	28	scheme	scheme	NOUN
eurjchem-1783	212	29	3	3	NUM
eurjchem-1783	212	30	)	)	PUNCT
eurjchem-1783	212	31	.	.	PUNCT
eurjchem-1783	213	1	color	color	NOUN
eurjchem-1783	213	2	:	:	PUNCT
eurjchem-1783	213	3	yellow	yellow	ADJ
eurjchem-1783	213	4	.	.	PUNCT
eurjchem-1783	214	1	yield	yield	NOUN
eurjchem-1783	214	2	:	:	PUNCT
eurjchem-1783	214	3	98	98	NUM
eurjchem-1783	214	4	%	%	NOUN
eurjchem-1783	214	5	.	.	PUNCT
eurjchem-1783	215	1	m.p	m.p	PROPN
eurjchem-1783	215	2	.	.	PROPN
eurjchem-1783	215	3	:	:	PUNCT
eurjchem-1783	216	1	112	112	NUM
eurjchem-1783	216	2	-	-	SYM
eurjchem-1783	216	3	113	113	NUM
eurjchem-1783	216	4	°	°	NOUN
eurjchem-1783	216	5	c	c	NOUN
eurjchem-1783	216	6	.	.	PUNCT
eurjchem-1783	217	1	1h	1h	NUM
eurjchem-1783	217	2	nmr	nmr	NOUN
eurjchem-1783	217	3	(	(	PUNCT
eurjchem-1783	217	4	400	400	NUM
eurjchem-1783	217	5	mhz	mhz	NOUN
eurjchem-1783	217	6	,	,	PUNCT
eurjchem-1783	217	7	cdcl3	cdcl3	PROPN
eurjchem-1783	217	8	,	,	PUNCT
eurjchem-1783	217	9	δ	δ	PROPN
eurjchem-1783	217	10	,	,	PUNCT
eurjchem-1783	217	11	ppm	ppm	NUM
eurjchem-1783	217	12	):	):	PUNCT
eurjchem-1783	217	13	6.78	6.78	NUM
eurjchem-1783	217	14	(	(	PUNCT
eurjchem-1783	217	15	t	t	PROPN
eurjchem-1783	217	16	,	,	PUNCT
eurjchem-1783	217	17	j	j	PROPN
eurjchem-1783	217	18	=	=	SYM
eurjchem-1783	217	19	8.8	8.8	NUM
eurjchem-1783	217	20	hz	hz	NOUN
eurjchem-1783	217	21	,	,	PUNCT
eurjchem-1783	217	22	1h	1h	NUM
eurjchem-1783	217	23	,	,	PUNCT
eurjchem-1783	217	24	ar	ar	NOUN
eurjchem-1783	217	25	-	-	NOUN
eurjchem-1783	217	26	h	h	NOUN
eurjchem-1783	217	27	)	)	PUNCT
eurjchem-1783	217	28	,	,	PUNCT
eurjchem-1783	217	29	6.38	6.38	NUM
eurjchem-1783	217	30	-	-	SYM
eurjchem-1783	217	31	6.45	6.45	NUM
eurjchem-1783	217	32	(	(	PUNCT
eurjchem-1783	217	33	m	m	PROPN
eurjchem-1783	217	34	,	,	PUNCT
eurjchem-1783	217	35	2h	2h	NUM
eurjchem-1783	217	36	,	,	PUNCT
eurjchem-1783	217	37	ar	ar	NOUN
eurjchem-1783	217	38	-	-	NOUN
eurjchem-1783	217	39	h	h	NOUN
eurjchem-1783	217	40	)	)	PUNCT
eurjchem-1783	217	41	,	,	PUNCT
eurjchem-1783	217	42	3.56	3.56	NUM
eurjchem-1783	217	43	(	(	PUNCT
eurjchem-1783	217	44	t	t	PROPN
eurjchem-1783	217	45	,	,	PUNCT
eurjchem-1783	217	46	j	j	PROPN
eurjchem-1783	218	1	=	=	PROPN
eurjchem-1783	218	2	4.48	4.48	NUM
eurjchem-1783	218	3	hz	hz	NOUN
eurjchem-1783	218	4	,	,	PUNCT
eurjchem-1783	218	5	4h	4h	NOUN
eurjchem-1783	218	6	,	,	PUNCT
eurjchem-1783	218	7	piperazine	piperazine	NOUN
eurjchem-1783	218	8	-	-	PUNCT
eurjchem-1783	218	9	h	h	NOUN
eurjchem-1783	218	10	)	)	PUNCT
eurjchem-1783	218	11	,	,	PUNCT
eurjchem-1783	218	12	2.90	2.90	NUM
eurjchem-1783	218	13	(	(	PUNCT
eurjchem-1783	218	14	t	t	PROPN
eurjchem-1783	218	15	,	,	PUNCT
eurjchem-1783	218	16	j	j	PROPN
eurjchem-1783	218	17	=	=	PUNCT
eurjchem-1783	218	18	4.24	4.24	NUM
eurjchem-1783	218	19	hz	hz	NOUN
eurjchem-1783	218	20	,	,	PUNCT
eurjchem-1783	218	21	4h	4h	NOUN
eurjchem-1783	218	22	,	,	PUNCT
eurjchem-1783	218	23	piperazine	piperazine	NOUN
eurjchem-1783	218	24	-	-	PUNCT
eurjchem-1783	218	25	h	h	NOUN
eurjchem-1783	218	26	)	)	PUNCT
eurjchem-1783	218	27	,	,	PUNCT
eurjchem-1783	218	28	1.47	1.47	NUM
eurjchem-1783	218	29	(	(	PUNCT
eurjchem-1783	218	30	s	s	PROPN
eurjchem-1783	218	31	,	,	PUNCT
eurjchem-1783	218	32	9h	9h	NUM
eurjchem-1783	218	33	,	,	PUNCT
eurjchem-1783	218	34	boc	boc	NOUN
eurjchem-1783	218	35	-	-	NOUN
eurjchem-1783	218	36	h	h	NOUN
eurjchem-1783	218	37	)	)	PUNCT
eurjchem-1783	218	38	.	.	PUNCT
eurjchem-1783	219	1	13c	13c	NOUN
eurjchem-1783	219	2	nmr	nmr	NOUN
eurjchem-1783	219	3	(	(	PUNCT
eurjchem-1783	219	4	100	100	NUM
eurjchem-1783	219	5	mhz	mhz	NOUN
eurjchem-1783	219	6	,	,	PUNCT
eurjchem-1783	219	7	cdcl3	cdcl3	PROPN
eurjchem-1783	219	8	,	,	PUNCT
eurjchem-1783	219	9	δ	δ	PROPN
eurjchem-1783	219	10	,	,	PUNCT
eurjchem-1783	219	11	ppm	ppm	NUM
eurjchem-1783	219	12	):	):	PUNCT
eurjchem-1783	219	13	154.5	154.5	NUM
eurjchem-1783	219	14	(	(	PUNCT
eurjchem-1783	219	15	1c	1c	NOUN
eurjchem-1783	219	16	,	,	PUNCT
eurjchem-1783	219	17	co	co	NOUN
eurjchem-1783	219	18	)	)	PUNCT
eurjchem-1783	219	19	,	,	PUNCT
eurjchem-1783	219	20	144.5	144.5	NUM
eurjchem-1783	219	21	(	(	PUNCT
eurjchem-1783	219	22	1c	1c	NOUN
eurjchem-1783	219	23	,	,	PUNCT
eurjchem-1783	219	24	ar	ar	NOUN
eurjchem-1783	219	25	-	-	NOUN
eurjchem-1783	219	26	c	c	NOUN
eurjchem-1783	219	27	)	)	PUNCT
eurjchem-1783	219	28	,	,	PUNCT
eurjchem-1783	219	29	139.86	139.86	NUM
eurjchem-1783	219	30	(	(	PUNCT
eurjchem-1783	219	31	1c	1c	X
eurjchem-1783	219	32	,	,	PUNCT
eurjchem-1783	219	33	ar	ar	NOUN
eurjchem-1783	219	34	-	-	NOUN
eurjchem-1783	219	35	c	c	NOUN
eurjchem-1783	219	36	)	)	PUNCT
eurjchem-1783	219	37	,	,	PUNCT
eurjchem-1783	219	38	119.2	119.2	NUM
eurjchem-1783	219	39	(	(	PUNCT
eurjchem-1783	219	40	2c	2c	NUM
eurjchem-1783	219	41	,	,	PUNCT
eurjchem-1783	219	42	ar	ar	NOUN
eurjchem-1783	219	43	-	-	NOUN
eurjchem-1783	219	44	c	c	NOUN
eurjchem-1783	219	45	)	)	PUNCT
eurjchem-1783	219	46	,	,	PUNCT
eurjchem-1783	219	47	116.4	116.4	NUM
eurjchem-1783	219	48	(	(	PUNCT
eurjchem-1783	219	49	2c	2c	NOUN
eurjchem-1783	219	50	,	,	PUNCT
eurjchem-1783	219	51	ar	ar	NOUN
eurjchem-1783	219	52	-	-	NOUN
eurjchem-1783	219	53	c	c	NOUN
eurjchem-1783	219	54	)	)	PUNCT
eurjchem-1783	219	55	,	,	PUNCT
eurjchem-1783	219	56	79.6	79.6	NUM
eurjchem-1783	219	57	(	(	PUNCT
eurjchem-1783	219	58	1c	1c	NOUN
eurjchem-1783	219	59	,	,	PUNCT
eurjchem-1783	219	60	c	c	NOUN
eurjchem-1783	219	61	-	-	PUNCT
eurjchem-1783	219	62	ch3	ch3	NOUN
eurjchem-1783	219	63	)	)	PUNCT
eurjchem-1783	219	64	,	,	PUNCT
eurjchem-1783	219	65	50	50	NUM
eurjchem-1783	219	66	(	(	PUNCT
eurjchem-1783	219	67	2c	2c	NOUN
eurjchem-1783	219	68	,	,	PUNCT
eurjchem-1783	219	69	piperazine	piperazine	NOUN
eurjchem-1783	219	70	-	-	PUNCT
eurjchem-1783	219	71	c	c	NOUN
eurjchem-1783	219	72	)	)	PUNCT
eurjchem-1783	219	73	,	,	PUNCT
eurjchem-1783	219	74	51.2	51.2	NUM
eurjchem-1783	219	75	(	(	PUNCT
eurjchem-1783	219	76	2c	2c	NOUN
eurjchem-1783	219	77	,	,	PUNCT
eurjchem-1783	219	78	piperazine	piperazine	NOUN
eurjchem-1783	219	79	-	-	PUNCT
eurjchem-1783	219	80	c	c	NOUN
eurjchem-1783	219	81	)	)	PUNCT
eurjchem-1783	219	82	,	,	PUNCT
eurjchem-1783	219	83	28.5	28.5	NUM
eurjchem-1783	219	84	(	(	PUNCT
eurjchem-1783	219	85	3c	3c	NUM
eurjchem-1783	219	86	,	,	PUNCT
eurjchem-1783	219	87	ch3	ch3	PROPN
eurjchem-1783	219	88	)	)	PUNCT
eurjchem-1783	219	89	.	.	PUNCT
eurjchem-1783	220	1	ms	ms	NOUN
eurjchem-1783	220	2	(	(	PUNCT
eurjchem-1783	220	3	m	m	PROPN
eurjchem-1783	220	4	/	/	SYM
eurjchem-1783	220	5	z	z	NOUN
eurjchem-1783	220	6	):	):	PUNCT
eurjchem-1783	220	7	296.2	296.2	NUM
eurjchem-1783	220	8	(	(	PUNCT
eurjchem-1783	220	9	m+	m+	NUM
eurjchem-1783	220	10	)	)	PUNCT
eurjchem-1783	220	11	.	.	PUNCT
eurjchem-1783	221	1	anal	anal	PROPN
eurjchem-1783	221	2	.	.	PUNCT
eurjchem-1783	221	3	calcd	calcd	NOUN
eurjchem-1783	221	4	.	.	PUNCT
eurjchem-1783	222	1	for	for	SCONJ
eurjchem-1783	222	2	c15h22fn3o2	c15h22fn3o2	PROPN
eurjchem-1783	222	3	:	:	PUNCT
eurjchem-1783	222	4	c	c	NOUN
eurjchem-1783	222	5	,	,	PUNCT
eurjchem-1783	222	6	61.00	61.00	NUM
eurjchem-1783	222	7	;	;	PUNCT
eurjchem-1783	222	8	h	h	X
eurjchem-1783	222	9	,	,	PUNCT
eurjchem-1783	222	10	7.51	7.51	NUM
eurjchem-1783	222	11	;	;	PUNCT
eurjchem-1783	222	12	n	n	CCONJ
eurjchem-1783	222	13	,	,	PUNCT
eurjchem-1783	222	14	14.23	14.23	NUM
eurjchem-1783	222	15	.	.	PUNCT
eurjchem-1783	222	16	found	find	VERB
eurjchem-1783	222	17	:	:	PUNCT
eurjchem-1783	223	1	c	c	X
eurjchem-1783	223	2	,	,	PUNCT
eurjchem-1783	223	3	61.22	61.22	NUM
eurjchem-1783	223	4	;	;	PUNCT
eurjchem-1783	223	5	h	h	X
eurjchem-1783	223	6	,	,	PUNCT
eurjchem-1783	223	7	7.62	7.62	NUM
eurjchem-1783	223	8	;	;	PUNCT
eurjchem-1783	223	9	n	n	CCONJ
eurjchem-1783	223	10	,	,	PUNCT
eurjchem-1783	223	11	14.21	14.21	NUM
eurjchem-1783	223	12	%	%	NOUN
eurjchem-1783	223	13	.	.	PUNCT
eurjchem-1783	224	1	2.2.9	2.2.9	X
eurjchem-1783	224	2	.	.	PUNCT
eurjchem-1783	225	1	synthesis	synthesis	NOUN
eurjchem-1783	225	2	of	of	ADP
eurjchem-1783	225	3	tert	tert	NOUN
eurjchem-1783	225	4	-	-	PUNCT
eurjchem-1783	225	5	butyl	butyl	NOUN
eurjchem-1783	225	6	4-(4-(((benzyloxy	4-(4-(((benzyloxy	NOUN
eurjchem-1783	225	7	)	)	PUNCT
eurjchem-1783	225	8	carbonyl	carbonyl	NOUN
eurjchem-1783	225	9	)	)	PUNCT
eurjchem-1783	225	10	amino)-2	amino)-2	PROPN
eurjchem-1783	225	11	-	-	PUNCT
eurjchem-1783	225	12	fluorophenyl	fluorophenyl	NOUN
eurjchem-1783	225	13	)	)	PUNCT
eurjchem-1783	225	14	piperazine-1	piperazine-1	NOUN
eurjchem-1783	225	15	-	-	NOUN
eurjchem-1783	225	16	carboxylate	carboxylate	NOUN
eurjchem-1783	225	17	(	(	PUNCT
eurjchem-1783	225	18	9	9	NUM
eurjchem-1783	225	19	)	)	PUNCT
eurjchem-1783	225	20	tert	tert	NOUN
eurjchem-1783	225	21	-	-	PUNCT
eurjchem-1783	225	22	butyl	butyl	NOUN
eurjchem-1783	225	23	4-(4	4-(4	NOUN
eurjchem-1783	225	24	-	-	PUNCT
eurjchem-1783	225	25	amino-2	amino-2	VERB
eurjchem-1783	225	26	-	-	PUNCT
eurjchem-1783	225	27	fluorophenyl	fluorophenyl	NOUN
eurjchem-1783	225	28	)	)	PUNCT
eurjchem-1783	225	29	piperazine-1	piperazine-1	NOUN
eurjchem-1783	225	30	-	-	NOUN
eurjchem-1783	225	31	carboxylate	carboxylate	NOUN
eurjchem-1783	225	32	(	(	PUNCT
eurjchem-1783	225	33	20	20	NUM
eurjchem-1783	225	34	g	g	NOUN
eurjchem-1783	225	35	,	,	PUNCT
eurjchem-1783	225	36	0.067	0.067	NUM
eurjchem-1783	225	37	mol	mol	NOUN
eurjchem-1783	225	38	)	)	PUNCT
eurjchem-1783	225	39	was	be	AUX
eurjchem-1783	225	40	dissolved	dissolve	VERB
eurjchem-1783	225	41	in	in	ADP
eurjchem-1783	225	42	dry	dry	ADJ
eurjchem-1783	225	43	thf	thf	NOUN
eurjchem-1783	225	44	(	(	PUNCT
eurjchem-1783	225	45	150	150	NUM
eurjchem-1783	225	46	ml	ml	NOUN
eurjchem-1783	225	47	)	)	PUNCT
eurjchem-1783	225	48	.	.	PUNCT
eurjchem-1783	226	1	added	add	VERB
eurjchem-1783	226	2	triethyl	triethyl	PROPN
eurjchem-1783	226	3	amine	amine	PROPN
eurjchem-1783	226	4	(	(	PUNCT
eurjchem-1783	226	5	11.33	11.33	NUM
eurjchem-1783	226	6	ml	ml	NOUN
eurjchem-1783	226	7	,	,	PUNCT
eurjchem-1783	226	8	0.081	0.081	NUM
eurjchem-1783	226	9	mol	mol	NOUN
eurjchem-1783	226	10	)	)	PUNCT
eurjchem-1783	226	11	and	and	CCONJ
eurjchem-1783	226	12	cooled	cool	VERB
eurjchem-1783	226	13	to	to	ADP
eurjchem-1783	226	14	-10	-10	PUNCT
eurjchem-1783	226	15	°	°	PRON
eurjchem-1783	226	16	c	c	NOUN
eurjchem-1783	226	17	.	.	PUNCT
eurjchem-1783	226	18	benzyl	benzyl	NOUN
eurjchem-1783	226	19	chloroformate	chloroformate	NOUN
eurjchem-1783	226	20	(	(	PUNCT
eurjchem-1783	226	21	10.55	10.55	NUM
eurjchem-1783	226	22	ml	ml	NOUN
eurjchem-1783	226	23	,	,	PUNCT
eurjchem-1783	226	24	0.074	0.074	NUM
eurjchem-1783	226	25	mol	mol	NOUN
eurjchem-1783	226	26	)	)	PUNCT
eurjchem-1783	226	27	diluted	dilute	VERB
eurjchem-1783	226	28	with	with	ADP
eurjchem-1783	226	29	thf	thf	NOUN
eurjchem-1783	226	30	(	(	PUNCT
eurjchem-1783	226	31	50	50	NUM
eurjchem-1783	226	32	ml	ml	NOUN
eurjchem-1783	226	33	)	)	PUNCT
eurjchem-1783	226	34	was	be	AUX
eurjchem-1783	226	35	slowly	slowly	ADV
eurjchem-1783	226	36	added	add	VERB
eurjchem-1783	226	37	in	in	ADP
eurjchem-1783	226	38	to	to	ADP
eurjchem-1783	226	39	the	the	DET
eurjchem-1783	226	40	flask	flask	NOUN
eurjchem-1783	226	41	by	by	ADP
eurjchem-1783	226	42	keeping	keep	VERB
eurjchem-1783	226	43	the	the	DET
eurjchem-1783	226	44	temperature	temperature	NOUN
eurjchem-1783	226	45	below	below	ADP
eurjchem-1783	226	46	0	0	NUM
eurjchem-1783	227	1	°	°	DET
eurjchem-1783	227	2	c	c	NOUN
eurjchem-1783	227	3	.	.	PUNCT
eurjchem-1783	228	1	after	after	SCONJ
eurjchem-1783	228	2	the	the	DET
eurjchem-1783	228	3	completion	completion	NOUN
eurjchem-1783	228	4	of	of	ADP
eurjchem-1783	228	5	addition	addition	NOUN
eurjchem-1783	228	6	cooling	cool	VERB
eurjchem-1783	228	7	bath	bath	NOUN
eurjchem-1783	228	8	was	be	AUX
eurjchem-1783	228	9	removed	remove	VERB
eurjchem-1783	228	10	and	and	CCONJ
eurjchem-1783	228	11	reaction	reaction	NOUN
eurjchem-1783	228	12	mixture	mixture	NOUN
eurjchem-1783	228	13	was	be	AUX
eurjchem-1783	228	14	warmed	warm	VERB
eurjchem-1783	228	15	to	to	ADP
eurjchem-1783	228	16	room	room	NOUN
eurjchem-1783	228	17	temperature	temperature	NOUN
eurjchem-1783	228	18	and	and	CCONJ
eurjchem-1783	228	19	stirred	stir	VERB
eurjchem-1783	228	20	at	at	ADP
eurjchem-1783	228	21	the	the	DET
eurjchem-1783	228	22	same	same	ADJ
eurjchem-1783	228	23	for	for	ADP
eurjchem-1783	228	24	1	1	NUM
eurjchem-1783	228	25	hr	hr	NOUN
eurjchem-1783	228	26	.	.	PUNCT
eurjchem-1783	229	1	completion	completion	NOUN
eurjchem-1783	229	2	of	of	ADP
eurjchem-1783	229	3	reaction	reaction	NOUN
eurjchem-1783	229	4	is	be	AUX
eurjchem-1783	229	5	monitored	monitor	VERB
eurjchem-1783	229	6	by	by	ADP
eurjchem-1783	229	7	tlc	tlc	PROPN
eurjchem-1783	229	8	.	.	PUNCT
eurjchem-1783	230	1	ethyl	ethyl	PROPN
eurjchem-1783	230	2	acetate	acetate	PROPN
eurjchem-1783	230	3	(	(	PUNCT
eurjchem-1783	230	4	100	100	NUM
eurjchem-1783	230	5	ml	ml	NOUN
eurjchem-1783	230	6	)	)	PUNCT
eurjchem-1783	230	7	and	and	CCONJ
eurjchem-1783	230	8	water	water	NOUN
eurjchem-1783	230	9	(	(	PUNCT
eurjchem-1783	230	10	100	100	NUM
eurjchem-1783	230	11	ml	ml	NOUN
eurjchem-1783	230	12	)	)	PUNCT
eurjchem-1783	230	13	were	be	AUX
eurjchem-1783	230	14	added	add	VERB
eurjchem-1783	230	15	,	,	PUNCT
eurjchem-1783	230	16	organic	organic	ADJ
eurjchem-1783	230	17	layer	layer	NOUN
eurjchem-1783	230	18	was	be	AUX
eurjchem-1783	230	19	separated	separate	VERB
eurjchem-1783	230	20	,	,	PUNCT
eurjchem-1783	230	21	and	and	CCONJ
eurjchem-1783	230	22	aqueous	aqueous	ADJ
eurjchem-1783	230	23	layer	layer	NOUN
eurjchem-1783	230	24	was	be	AUX
eurjchem-1783	230	25	extracted	extract	VERB
eurjchem-1783	230	26	with	with	ADP
eurjchem-1783	230	27	ethyl	ethyl	PROPN
eurjchem-1783	230	28	acetate	acetate	NOUN
eurjchem-1783	230	29	(	(	PUNCT
eurjchem-1783	230	30	2×50	2×50	NUM
eurjchem-1783	230	31	ml	ml	NOUN
eurjchem-1783	230	32	)	)	PUNCT
eurjchem-1783	230	33	,	,	PUNCT
eurjchem-1783	230	34	combined	combine	VERB
eurjchem-1783	230	35	organic	organic	ADJ
eurjchem-1783	230	36	layer	layer	NOUN
eurjchem-1783	230	37	was	be	AUX
eurjchem-1783	230	38	washed	wash	VERB
eurjchem-1783	230	39	with	with	ADP
eurjchem-1783	230	40	water	water	NOUN
eurjchem-1783	230	41	(	(	PUNCT
eurjchem-1783	230	42	2×50	2×50	NUM
eurjchem-1783	230	43	ml	ml	NOUN
eurjchem-1783	230	44	)	)	PUNCT
eurjchem-1783	230	45	,	,	PUNCT
eurjchem-1783	230	46	brine	brine	NOUN
eurjchem-1783	230	47	(	(	PUNCT
eurjchem-1783	230	48	50	50	NUM
eurjchem-1783	230	49	ml	ml	NOUN
eurjchem-1783	230	50	)	)	PUNCT
eurjchem-1783	230	51	,	,	PUNCT
eurjchem-1783	230	52	dried	dry	VERB
eurjchem-1783	230	53	over	over	ADP
eurjchem-1783	230	54	na2so4	na2so4	NOUN
eurjchem-1783	230	55	,	,	PUNCT
eurjchem-1783	230	56	filtered	filter	VERB
eurjchem-1783	230	57	and	and	CCONJ
eurjchem-1783	230	58	concentrated	concentrate	VERB
eurjchem-1783	230	59	to	to	PART
eurjchem-1783	230	60	obtain	obtain	VERB
eurjchem-1783	230	61	the	the	DET
eurjchem-1783	230	62	crude	crude	ADJ
eurjchem-1783	230	63	product	product	NOUN
eurjchem-1783	230	64	.	.	PUNCT
eurjchem-1783	231	1	crude	crude	ADJ
eurjchem-1783	231	2	product	product	NOUN
eurjchem-1783	231	3	obtained	obtain	VERB
eurjchem-1783	231	4	was	be	AUX
eurjchem-1783	231	5	added	add	VERB
eurjchem-1783	231	6	hexane	hexane	NOUN
eurjchem-1783	231	7	:	:	PUNCT
eurjchem-1783	231	8	diethyl	diethyl	NOUN
eurjchem-1783	231	9	ether	ether	NOUN
eurjchem-1783	231	10	(	(	PUNCT
eurjchem-1783	231	11	9:1	9:1	NUM
eurjchem-1783	231	12	,	,	PUNCT
eurjchem-1783	231	13	v	v	NOUN
eurjchem-1783	231	14	:	:	PUNCT
eurjchem-1783	231	15	v	v	NOUN
eurjchem-1783	231	16	,	,	PUNCT
eurjchem-1783	231	17	3×100	3×100	NUM
eurjchem-1783	231	18	ml	ml	NOUN
eurjchem-1783	231	19	)	)	PUNCT
eurjchem-1783	231	20	and	and	CCONJ
eurjchem-1783	231	21	stirred	stir	VERB
eurjchem-1783	231	22	for	for	ADP
eurjchem-1783	231	23	10	10	NUM
eurjchem-1783	231	24	mins	min	NOUN
eurjchem-1783	231	25	.	.	PUNCT
eurjchem-1783	232	1	filtered	filter	VERB
eurjchem-1783	232	2	and	and	CCONJ
eurjchem-1783	232	3	dried	dry	VERB
eurjchem-1783	232	4	to	to	PART
eurjchem-1783	232	5	get	get	VERB
eurjchem-1783	232	6	a	a	DET
eurjchem-1783	232	7	pure	pure	ADJ
eurjchem-1783	232	8	product	product	NOUN
eurjchem-1783	232	9	as	as	ADP
eurjchem-1783	232	10	off	off	ADP
eurjchem-1783	232	11	white	white	ADJ
eurjchem-1783	232	12	solid	solid	ADJ
eurjchem-1783	232	13	(	(	PUNCT
eurjchem-1783	232	14	scheme	scheme	NOUN
eurjchem-1783	232	15	3	3	NUM
eurjchem-1783	232	16	)	)	PUNCT
eurjchem-1783	232	17	.	.	PUNCT
eurjchem-1783	233	1	color	color	NOUN
eurjchem-1783	233	2	:	:	PUNCT
eurjchem-1783	233	3	off	off	ADP
eurjchem-1783	233	4	white	white	PROPN
eurjchem-1783	233	5	.	.	PUNCT
eurjchem-1783	234	1	yield	yield	NOUN
eurjchem-1783	234	2	:	:	PUNCT
eurjchem-1783	234	3	98	98	NUM
eurjchem-1783	234	4	%	%	NOUN
eurjchem-1783	234	5	.	.	PUNCT
eurjchem-1783	235	1	m.p	m.p	PROPN
eurjchem-1783	235	2	.	.	PROPN
eurjchem-1783	235	3	:	:	PUNCT
eurjchem-1783	236	1	249	249	NUM
eurjchem-1783	236	2	-	-	SYM
eurjchem-1783	236	3	250	250	NUM
eurjchem-1783	236	4	°	°	NUM
eurjchem-1783	236	5	c	c	NOUN
eurjchem-1783	236	6	.	.	PUNCT
eurjchem-1783	237	1	1h	1h	NUM
eurjchem-1783	237	2	nmr	nmr	NOUN
eurjchem-1783	237	3	(	(	PUNCT
eurjchem-1783	237	4	400	400	NUM
eurjchem-1783	237	5	mhz	mhz	NOUN
eurjchem-1783	237	6	,	,	PUNCT
eurjchem-1783	237	7	cdcl3	cdcl3	PROPN
eurjchem-1783	237	8	,	,	PUNCT
eurjchem-1783	237	9	δ	δ	PROPN
eurjchem-1783	237	10	,	,	PUNCT
eurjchem-1783	237	11	ppm	ppm	NUM
eurjchem-1783	237	12	):	):	PUNCT
eurjchem-1783	237	13	7.36	7.36	NUM
eurjchem-1783	237	14	(	(	PUNCT
eurjchem-1783	237	15	m	m	PROPN
eurjchem-1783	237	16	,	,	PUNCT
eurjchem-1783	237	17	5h	5h	NUM
eurjchem-1783	237	18	,	,	PUNCT
eurjchem-1783	237	19	ar	ar	NOUN
eurjchem-1783	237	20	-	-	NOUN
eurjchem-1783	237	21	h	h	NOUN
eurjchem-1783	237	22	)	)	PUNCT
eurjchem-1783	237	23	,	,	PUNCT
eurjchem-1783	237	24	6.97	6.97	NUM
eurjchem-1783	237	25	(	(	PUNCT
eurjchem-1783	237	26	d	d	PROPN
eurjchem-1783	237	27	,	,	PUNCT
eurjchem-1783	237	28	j	j	PROPN
eurjchem-1783	237	29	=	=	SYM
eurjchem-1783	237	30	7.3	7.3	NUM
eurjchem-1783	237	31	hz	hz	NOUN
eurjchem-1783	237	32	,	,	PUNCT
eurjchem-1783	237	33	1h	1h	NUM
eurjchem-1783	237	34	,	,	PUNCT
eurjchem-1783	237	35	ar	ar	NOUN
eurjchem-1783	237	36	-	-	NOUN
eurjchem-1783	237	37	h	h	NOUN
eurjchem-1783	237	38	)	)	PUNCT
eurjchem-1783	237	39	,	,	PUNCT
eurjchem-1783	237	40	6.87	6.87	NUM
eurjchem-1783	237	41	(	(	PUNCT
eurjchem-1783	237	42	t	t	PROPN
eurjchem-1783	237	43	,	,	PUNCT
eurjchem-1783	237	44	j	j	PROPN
eurjchem-1783	238	1	=	=	SYM
eurjchem-1783	238	2	8.9	8.9	NUM
eurjchem-1783	238	3	hz	hz	NOUN
eurjchem-1783	238	4	,	,	PUNCT
eurjchem-1783	238	5	1h	1h	NUM
eurjchem-1783	238	6	,	,	PUNCT
eurjchem-1783	238	7	ar	ar	NOUN
eurjchem-1783	238	8	-	-	NOUN
eurjchem-1783	238	9	h	h	NOUN
eurjchem-1783	238	10	)	)	PUNCT
eurjchem-1783	238	11	,	,	PUNCT
eurjchem-1783	238	12	6.72	6.72	NUM
eurjchem-1783	238	13	(	(	PUNCT
eurjchem-1783	238	14	s	s	PROPN
eurjchem-1783	238	15	,	,	PUNCT
eurjchem-1783	238	16	1h	1h	NUM
eurjchem-1783	238	17	,	,	PUNCT
eurjchem-1783	238	18	ar	ar	NOUN
eurjchem-1783	238	19	-	-	NOUN
eurjchem-1783	238	20	h	h	NOUN
eurjchem-1783	238	21	)	)	PUNCT
eurjchem-1783	238	22	,	,	PUNCT
eurjchem-1783	238	23	5.17	5.17	NUM
eurjchem-1783	238	24	(	(	PUNCT
eurjchem-1783	238	25	s	s	PROPN
eurjchem-1783	238	26	,	,	PUNCT
eurjchem-1783	238	27	2h	2h	NUM
eurjchem-1783	238	28	,	,	PUNCT
eurjchem-1783	238	29	ch2	ch2	PROPN
eurjchem-1783	238	30	)	)	PUNCT
eurjchem-1783	238	31	,	,	PUNCT
eurjchem-1783	238	32	3.68	3.68	NUM
eurjchem-1783	238	33	(	(	PUNCT
eurjchem-1783	238	34	t	t	PROPN
eurjchem-1783	238	35	,	,	PUNCT
eurjchem-1783	238	36	j	j	PROPN
eurjchem-1783	239	1	=	=	SYM
eurjchem-1783	239	2	5.0	5.0	NUM
eurjchem-1783	239	3	hz	hz	NOUN
eurjchem-1783	239	4	,	,	PUNCT
eurjchem-1783	239	5	4h	4h	NOUN
eurjchem-1783	239	6	,	,	PUNCT
eurjchem-1783	239	7	piperazine	piperazine	NOUN
eurjchem-1783	239	8	-	-	PUNCT
eurjchem-1783	239	9	h	h	NOUN
eurjchem-1783	239	10	)	)	PUNCT
eurjchem-1783	239	11	,	,	PUNCT
eurjchem-1783	239	12	3.00	3.00	NUM
eurjchem-1783	239	13	(	(	PUNCT
eurjchem-1783	239	14	brd	brd	PROPN
eurjchem-1783	239	15	,	,	PUNCT
eurjchem-1783	239	16	4h	4h	NOUN
eurjchem-1783	239	17	,	,	PUNCT
eurjchem-1783	239	18	piperazine	piperazine	NOUN
eurjchem-1783	239	19	-	-	PUNCT
eurjchem-1783	239	20	h	h	NOUN
eurjchem-1783	239	21	)	)	PUNCT
eurjchem-1783	239	22	,	,	PUNCT
eurjchem-1783	239	23	1.47	1.47	NUM
eurjchem-1783	239	24	(	(	PUNCT
eurjchem-1783	239	25	s	s	PROPN
eurjchem-1783	239	26	,	,	PUNCT
eurjchem-1783	239	27	9h	9h	NUM
eurjchem-1783	239	28	,	,	PUNCT
eurjchem-1783	239	29	boc	boc	NOUN
eurjchem-1783	239	30	-	-	NOUN
eurjchem-1783	239	31	h	h	NOUN
eurjchem-1783	239	32	)	)	PUNCT
eurjchem-1783	239	33	.	.	PUNCT
eurjchem-1783	240	1	13c	13c	NOUN
eurjchem-1783	240	2	nmr	nmr	NOUN
eurjchem-1783	240	3	(	(	PUNCT
eurjchem-1783	240	4	100	100	NUM
eurjchem-1783	240	5	mhz	mhz	NOUN
eurjchem-1783	240	6	,	,	PUNCT
eurjchem-1783	240	7	cdcl3	cdcl3	PROPN
eurjchem-1783	240	8	,	,	PUNCT
eurjchem-1783	240	9	δ	δ	PROPN
eurjchem-1783	240	10	,	,	PUNCT
eurjchem-1783	240	11	ppm	ppm	NOUN
eurjchem-1783	240	12	):	):	PUNCT
eurjchem-1783	240	13	156.0	156.0	NUM
eurjchem-1783	240	14	(	(	PUNCT
eurjchem-1783	240	15	1c	1c	NOUN
eurjchem-1783	240	16	,	,	PUNCT
eurjchem-1783	240	17	arnhco	arnhco	ADJ
eurjchem-1783	240	18	)	)	PUNCT
eurjchem-1783	240	19	,	,	PUNCT
eurjchem-1783	240	20	154.3	154.3	NUM
eurjchem-1783	240	21	(	(	PUNCT
eurjchem-1783	240	22	1c	1c	NOUN
eurjchem-1783	240	23	,	,	PUNCT
eurjchem-1783	240	24	co	co	NOUN
eurjchem-1783	240	25	)	)	PUNCT
eurjchem-1783	240	26	,	,	PUNCT
eurjchem-1783	240	27	147.6	147.6	NUM
eurjchem-1783	240	28	(	(	PUNCT
eurjchem-1783	240	29	1c	1c	NOUN
eurjchem-1783	240	30	,	,	PUNCT
eurjchem-1783	240	31	ar	ar	NOUN
eurjchem-1783	240	32	-	-	NOUN
eurjchem-1783	240	33	c	c	NOUN
eurjchem-1783	240	34	)	)	PUNCT
eurjchem-1783	240	35	,	,	PUNCT
eurjchem-1783	240	36	137.5	137.5	NUM
eurjchem-1783	240	37	(	(	PUNCT
eurjchem-1783	240	38	1c	1c	NOUN
eurjchem-1783	240	39	,	,	PUNCT
eurjchem-1783	240	40	ar	ar	NOUN
eurjchem-1783	240	41	-	-	NOUN
eurjchem-1783	240	42	c	c	NOUN
eurjchem-1783	240	43	)	)	PUNCT
eurjchem-1783	240	44	,	,	PUNCT
eurjchem-1783	240	45	136.2	136.2	NUM
eurjchem-1783	240	46	(	(	PUNCT
eurjchem-1783	240	47	1c	1c	NOUN
eurjchem-1783	240	48	,	,	PUNCT
eurjchem-1783	240	49	ar	ar	NOUN
eurjchem-1783	240	50	-	-	NOUN
eurjchem-1783	240	51	c	c	NOUN
eurjchem-1783	240	52	)	)	PUNCT
eurjchem-1783	240	53	,	,	PUNCT
eurjchem-1783	240	54	129.6	129.6	NUM
eurjchem-1783	240	55	(	(	PUNCT
eurjchem-1783	240	56	1c	1c	NOUN
eurjchem-1783	240	57	,	,	PUNCT
eurjchem-1783	240	58	ar	ar	NOUN
eurjchem-1783	240	59	-	-	ADJ
eurjchem-1783	240	60	c),128.8	c),128.8	ADJ
eurjchem-1783	240	61	(	(	PUNCT
eurjchem-1783	240	62	1c	1c	NOUN
eurjchem-1783	240	63	,	,	PUNCT
eurjchem-1783	240	64	ar	ar	NOUN
eurjchem-1783	240	65	-	-	NOUN
eurjchem-1783	240	66	c	c	NOUN
eurjchem-1783	240	67	)	)	PUNCT
eurjchem-1783	240	68	,	,	PUNCT
eurjchem-1783	240	69	128.4	128.4	NUM
eurjchem-1783	240	70	(	(	PUNCT
eurjchem-1783	240	71	2c	2c	NUM
eurjchem-1783	240	72	,	,	PUNCT
eurjchem-1783	240	73	ar	ar	NOUN
eurjchem-1783	240	74	-	-	NOUN
eurjchem-1783	240	75	c	c	NOUN
eurjchem-1783	240	76	)	)	PUNCT
eurjchem-1783	240	77	,	,	PUNCT
eurjchem-1783	240	78	127.9	127.9	NUM
eurjchem-1783	240	79	(	(	PUNCT
eurjchem-1783	240	80	2c	2c	NUM
eurjchem-1783	240	81	,	,	PUNCT
eurjchem-1783	240	82	ar	ar	NOUN
eurjchem-1783	240	83	-	-	NOUN
eurjchem-1783	240	84	c	c	NOUN
eurjchem-1783	240	85	)	)	PUNCT
eurjchem-1783	240	86	,	,	PUNCT
eurjchem-1783	240	87	127.7	127.7	NUM
eurjchem-1783	240	88	(	(	PUNCT
eurjchem-1783	240	89	1c	1c	NOUN
eurjchem-1783	240	90	,	,	PUNCT
eurjchem-1783	240	91	ar	ar	NOUN
eurjchem-1783	240	92	-	-	NOUN
eurjchem-1783	240	93	c	c	NOUN
eurjchem-1783	240	94	)	)	PUNCT
eurjchem-1783	240	95	,	,	PUNCT
eurjchem-1783	240	96	126.4	126.4	NUM
eurjchem-1783	240	97	(	(	PUNCT
eurjchem-1783	240	98	1c	1c	NOUN
eurjchem-1783	240	99	,	,	PUNCT
eurjchem-1783	240	100	ar	ar	NOUN
eurjchem-1783	240	101	-	-	NOUN
eurjchem-1783	240	102	c	c	NOUN
eurjchem-1783	240	103	)	)	PUNCT
eurjchem-1783	240	104	,	,	PUNCT
eurjchem-1783	240	105	120.2	120.2	NUM
eurjchem-1783	240	106	(	(	PUNCT
eurjchem-1783	240	107	1c	1c	NOUN
eurjchem-1783	240	108	,	,	PUNCT
eurjchem-1783	240	109	ar	ar	NOUN
eurjchem-1783	240	110	-	-	NOUN
eurjchem-1783	240	111	c	c	NOUN
eurjchem-1783	240	112	)	)	PUNCT
eurjchem-1783	240	113	,	,	PUNCT
eurjchem-1783	240	114	79.6	79.6	NUM
eurjchem-1783	240	115	(	(	PUNCT
eurjchem-1783	240	116	1c	1c	NOUN
eurjchem-1783	240	117	,	,	PUNCT
eurjchem-1783	240	118	c	c	NOUN
eurjchem-1783	240	119	-	-	PUNCT
eurjchem-1783	240	120	ch3	ch3	NOUN
eurjchem-1783	240	121	)	)	PUNCT
eurjchem-1783	240	122	,	,	PUNCT
eurjchem-1783	240	123	67.4	67.4	NUM
eurjchem-1783	240	124	(	(	PUNCT
eurjchem-1783	240	125	1c	1c	NOUN
eurjchem-1783	240	126	,	,	PUNCT
eurjchem-1783	240	127	ch2	ch2	PROPN
eurjchem-1783	240	128	)	)	PUNCT
eurjchem-1783	240	129	,	,	PUNCT
eurjchem-1783	240	130	53.1	53.1	NUM
eurjchem-1783	240	131	(	(	PUNCT
eurjchem-1783	240	132	2c	2c	NOUN
eurjchem-1783	240	133	,	,	PUNCT
eurjchem-1783	240	134	piperazine	piperazine	NOUN
eurjchem-1783	240	135	-	-	PUNCT
eurjchem-1783	240	136	c	c	NOUN
eurjchem-1783	240	137	)	)	PUNCT
eurjchem-1783	240	138	,	,	PUNCT
eurjchem-1783	240	139	51.1	51.1	NUM
eurjchem-1783	240	140	(	(	PUNCT
eurjchem-1783	240	141	2c	2c	NOUN
eurjchem-1783	240	142	,	,	PUNCT
eurjchem-1783	240	143	piperazine	piperazine	NOUN
eurjchem-1783	240	144	-	-	PUNCT
eurjchem-1783	240	145	c	c	NOUN
eurjchem-1783	240	146	)	)	PUNCT
eurjchem-1783	240	147	,	,	PUNCT
eurjchem-1783	240	148	28.6	28.6	NUM
eurjchem-1783	240	149	(	(	PUNCT
eurjchem-1783	240	150	3c	3c	NUM
eurjchem-1783	240	151	,	,	PUNCT
eurjchem-1783	240	152	ch3	ch3	PROPN
eurjchem-1783	240	153	)	)	PUNCT
eurjchem-1783	240	154	.	.	PUNCT
eurjchem-1783	241	1	ms	ms	NOUN
eurjchem-1783	241	2	(	(	PUNCT
eurjchem-1783	241	3	m	m	PROPN
eurjchem-1783	241	4	/	/	SYM
eurjchem-1783	241	5	z	z	NOUN
eurjchem-1783	241	6	):	):	PUNCT
eurjchem-1783	241	7	431.1	431.1	NUM
eurjchem-1783	241	8	(	(	PUNCT
eurjchem-1783	241	9	m+	m+	NUM
eurjchem-1783	241	10	)	)	PUNCT
eurjchem-1783	241	11	.	.	PUNCT
eurjchem-1783	242	1	anal	anal	PROPN
eurjchem-1783	242	2	.	.	PUNCT
eurjchem-1783	242	3	calcd	calcd	NOUN
eurjchem-1783	242	4	.	.	PUNCT
eurjchem-1783	243	1	for	for	ADP
eurjchem-1783	243	2	c23h28fn3o4	c23h28fn3o4	PROPN
eurjchem-1783	243	3	:	:	PUNCT
eurjchem-1783	243	4	c	c	X
eurjchem-1783	243	5	,	,	PUNCT
eurjchem-1783	243	6	64.32	64.32	NUM
eurjchem-1783	243	7	;	;	PUNCT
eurjchem-1783	243	8	h	h	NOUN
eurjchem-1783	243	9	,	,	PUNCT
eurjchem-1783	243	10	6.57	6.57	NUM
eurjchem-1783	243	11	;	;	PUNCT
eurjchem-1783	243	12	n	n	CCONJ
eurjchem-1783	243	13	,	,	PUNCT
eurjchem-1783	243	14	9.78	9.78	NUM
eurjchem-1783	243	15	.	.	PUNCT
eurjchem-1783	243	16	found	find	VERB
eurjchem-1783	243	17	:	:	PUNCT
eurjchem-1783	244	1	c	c	X
eurjchem-1783	244	2	,	,	PUNCT
eurjchem-1783	244	3	64.28	64.28	NUM
eurjchem-1783	244	4	;	;	PUNCT
eurjchem-1783	244	5	h	h	X
eurjchem-1783	244	6	,	,	PUNCT
eurjchem-1783	244	7	6.56	6.56	NUM
eurjchem-1783	244	8	;	;	PUNCT
eurjchem-1783	244	9	n	n	CCONJ
eurjchem-1783	244	10	,	,	PUNCT
eurjchem-1783	244	11	9.81	9.81	NUM
eurjchem-1783	244	12	%	%	NOUN
eurjchem-1783	244	13	.	.	PUNCT
eurjchem-1783	245	1	2.2.10	2.2.10	NUM
eurjchem-1783	245	2	.	.	PUNCT
eurjchem-1783	246	1	synthesis	synthesis	NOUN
eurjchem-1783	246	2	of	of	ADP
eurjchem-1783	246	3	(	(	PUNCT
eurjchem-1783	246	4	r)-tert	r)-tert	ADJ
eurjchem-1783	246	5	-	-	PUNCT
eurjchem-1783	246	6	butyl	butyl	ADJ
eurjchem-1783	246	7	4-(4-(5-(bromomethyl)-2oxooxazolidin-3	4-(4-(5-(bromomethyl)-2oxooxazolidin-3	PROPN
eurjchem-1783	246	8	-	-	PUNCT
eurjchem-1783	246	9	yl)-2	yl)-2	NOUN
eurjchem-1783	246	10	-	-	PUNCT
eurjchem-1783	246	11	fluorophenyl	fluorophenyl	NOUN
eurjchem-1783	246	12	)	)	PUNCT
eurjchem-1783	246	13	piperazine-1carboxylate	piperazine-1carboxylate	PROPN
eurjchem-1783	246	14	(	(	PUNCT
eurjchem-1783	246	15	10	10	NUM
eurjchem-1783	246	16	)	)	PUNCT
eurjchem-1783	246	17	benzyl(3	benzyl(3	NOUN
eurjchem-1783	246	18	-	-	PUNCT
eurjchem-1783	246	19	fluoro-4	fluoro-4	NOUN
eurjchem-1783	246	20	-	-	PUNCT
eurjchem-1783	246	21	morpholinophenyl)carbamate	morpholinophenyl)carbamate	NOUN
eurjchem-1783	246	22	(	(	PUNCT
eurjchem-1783	246	23	5	5	NUM
eurjchem-1783	246	24	g	g	NOUN
eurjchem-1783	246	25	,	,	PUNCT
eurjchem-1783	246	26	0.011	0.011	NUM
eurjchem-1783	246	27	mol	mol	NOUN
eurjchem-1783	246	28	)	)	PUNCT
eurjchem-1783	246	29	was	be	AUX
eurjchem-1783	246	30	dissolved	dissolve	VERB
eurjchem-1783	246	31	in	in	ADP
eurjchem-1783	246	32	dry	dry	ADJ
eurjchem-1783	246	33	acetonitrile	acetonitrile	NOUN
eurjchem-1783	246	34	(	(	PUNCT
eurjchem-1783	246	35	100	100	NUM
eurjchem-1783	246	36	ml	ml	NOUN
eurjchem-1783	246	37	)	)	PUNCT
eurjchem-1783	246	38	,	,	PUNCT
eurjchem-1783	246	39	added	add	VERB
eurjchem-1783	246	40	cesium	cesium	NOUN
eurjchem-1783	246	41	carbonate	carbonate	NOUN
eurjchem-1783	246	42	(	(	PUNCT
eurjchem-1783	246	43	5.69	5.69	NUM
eurjchem-1783	246	44	g	g	NOUN
eurjchem-1783	246	45	,	,	PUNCT
eurjchem-1783	246	46	0.017	0.017	NUM
eurjchem-1783	246	47	mol	mol	NOUN
eurjchem-1783	246	48	)	)	PUNCT
eurjchem-1783	246	49	,	,	PUNCT
eurjchem-1783	246	50	(	(	PUNCT
eurjchem-1783	246	51	r)-2-(bromomethyl	r)-2-(bromomethyl	NOUN
eurjchem-1783	246	52	)	)	PUNCT
eurjchem-1783	246	53	oxirane	oxirane	NOUN
eurjchem-1783	246	54	(	(	PUNCT
eurjchem-1783	246	55	1.74	1.74	NUM
eurjchem-1783	246	56	g	g	NOUN
eurjchem-1783	246	57	,	,	PUNCT
eurjchem-1783	246	58	0.012	0.012	NUM
eurjchem-1783	246	59	mol	mol	NOUN
eurjchem-1783	246	60	)	)	PUNCT
eurjchem-1783	246	61	through	through	ADP
eurjchem-1783	246	62	syringe	syringe	NOUN
eurjchem-1783	246	63	,	,	PUNCT
eurjchem-1783	246	64	stirred	stir	VERB
eurjchem-1783	246	65	at	at	ADP
eurjchem-1783	246	66	room	room	NOUN
eurjchem-1783	246	67	temperature	temperature	NOUN
eurjchem-1783	246	68	for	for	ADP
eurjchem-1783	246	69	10	10	NUM
eurjchem-1783	246	70	min	min	NOUN
eurjchem-1783	246	71	and	and	CCONJ
eurjchem-1783	246	72	refluxed	refluxe	VERB
eurjchem-1783	246	73	for	for	ADP
eurjchem-1783	246	74	5	5	NUM
eurjchem-1783	246	75	hr	hr	NOUN
eurjchem-1783	246	76	.	.	PUNCT
eurjchem-1783	247	1	reaction	reaction	NOUN
eurjchem-1783	247	2	was	be	AUX
eurjchem-1783	247	3	monitored	monitor	VERB
eurjchem-1783	247	4	by	by	ADP
eurjchem-1783	247	5	tlc	tlc	NOUN
eurjchem-1783	247	6	.	.	PUNCT
eurjchem-1783	248	1	reaction	reaction	NOUN
eurjchem-1783	248	2	mixture	mixture	NOUN
eurjchem-1783	248	3	was	be	AUX
eurjchem-1783	248	4	cooled	cool	VERB
eurjchem-1783	248	5	,	,	PUNCT
eurjchem-1783	248	6	filtered	filter	VERB
eurjchem-1783	248	7	,	,	PUNCT
eurjchem-1783	248	8	concentrated	concentrate	VERB
eurjchem-1783	248	9	to	to	PART
eurjchem-1783	248	10	obtain	obtain	VERB
eurjchem-1783	248	11	crude	crude	ADJ
eurjchem-1783	248	12	compound	compound	NOUN
eurjchem-1783	248	13	which	which	PRON
eurjchem-1783	248	14	was	be	AUX
eurjchem-1783	248	15	further	far	ADV
eurjchem-1783	248	16	purified	purify	VERB
eurjchem-1783	248	17	by	by	ADP
eurjchem-1783	248	18	flash	flash	NOUN
eurjchem-1783	248	19	column	column	NOUN
eurjchem-1783	248	20	chromatography	chromatography	NOUN
eurjchem-1783	248	21	using	use	VERB
eurjchem-1783	248	22	20	20	NUM
eurjchem-1783	248	23	-	-	SYM
eurjchem-1783	248	24	35	35	NUM
eurjchem-1783	248	25	%	%	NOUN
eurjchem-1783	248	26	ethyl	ethyl	PROPN
eurjchem-1783	248	27	acetate	acetate	NOUN
eurjchem-1783	248	28	in	in	ADP
eurjchem-1783	248	29	hexane	hexane	NOUN
eurjchem-1783	248	30	to	to	PART
eurjchem-1783	248	31	obtain	obtain	VERB
eurjchem-1783	248	32	the	the	DET
eurjchem-1783	248	33	product	product	NOUN
eurjchem-1783	248	34	as	as	ADP
eurjchem-1783	248	35	pale	pale	ADJ
eurjchem-1783	248	36	yellow	yellow	ADJ
eurjchem-1783	248	37	color	color	NOUN
eurjchem-1783	248	38	solid	solid	ADJ
eurjchem-1783	248	39	(	(	PUNCT
eurjchem-1783	248	40	scheme	scheme	NOUN
eurjchem-1783	248	41	3	3	NUM
eurjchem-1783	248	42	)	)	PUNCT
eurjchem-1783	248	43	.	.	PUNCT
eurjchem-1783	249	1	color	color	NOUN
eurjchem-1783	249	2	:	:	PUNCT
eurjchem-1783	249	3	pale	pale	ADJ
eurjchem-1783	249	4	yellow	yellow	ADJ
eurjchem-1783	249	5	.	.	PUNCT
eurjchem-1783	250	1	yield	yield	NOUN
eurjchem-1783	250	2	:	:	PUNCT
eurjchem-1783	250	3	95	95	NUM
eurjchem-1783	250	4	%	%	NOUN
eurjchem-1783	250	5	.	.	PUNCT
eurjchem-1783	251	1	m.p	m.p	PROPN
eurjchem-1783	251	2	.	.	PROPN
eurjchem-1783	251	3	:	:	PUNCT
eurjchem-1783	252	1	196	196	NUM
eurjchem-1783	252	2	-	-	SYM
eurjchem-1783	252	3	197	197	NUM
eurjchem-1783	252	4	°	°	NOUN
eurjchem-1783	252	5	c	c	NOUN
eurjchem-1783	252	6	.	.	PUNCT
eurjchem-1783	253	1	1h	1h	NUM
eurjchem-1783	253	2	nmr	nmr	NOUN
eurjchem-1783	253	3	(	(	PUNCT
eurjchem-1783	253	4	400	400	NUM
eurjchem-1783	253	5	mhz	mhz	NOUN
eurjchem-1783	253	6	,	,	PUNCT
eurjchem-1783	253	7	cdcl3	cdcl3	PROPN
eurjchem-1783	253	8	,	,	PUNCT
eurjchem-1783	253	9	δ	δ	PROPN
eurjchem-1783	253	10	,	,	PUNCT
eurjchem-1783	253	11	ppm	ppm	NUM
eurjchem-1783	253	12	):	):	PUNCT
eurjchem-1783	253	13	7.46	7.46	NUM
eurjchem-1783	253	14	(	(	PUNCT
eurjchem-1783	253	15	dd	dd	PROPN
eurjchem-1783	253	16	,	,	PUNCT
eurjchem-1783	253	17	j	j	PROPN
eurjchem-1783	253	18	=	=	PROPN
eurjchem-1783	253	19	13.52	13.52	NUM
eurjchem-1783	253	20	hz	hz	NOUN
eurjchem-1783	253	21	,	,	PUNCT
eurjchem-1783	253	22	1h	1h	NUM
eurjchem-1783	253	23	,	,	PUNCT
eurjchem-1783	253	24	ar	ar	NOUN
eurjchem-1783	253	25	-	-	NOUN
eurjchem-1783	253	26	h	h	NOUN
eurjchem-1783	253	27	)	)	PUNCT
eurjchem-1783	253	28	,	,	PUNCT
eurjchem-1783	253	29	7.26	7.26	NUM
eurjchem-1783	253	30	(	(	PUNCT
eurjchem-1783	253	31	dd	dd	PROPN
eurjchem-1783	253	32	,	,	PUNCT
eurjchem-1783	253	33	j	j	PROPN
eurjchem-1783	253	34	=	=	NOUN
eurjchem-1783	253	35	8.72	8.72	NUM
eurjchem-1783	253	36	hz	hz	NOUN
eurjchem-1783	253	37	,	,	PUNCT
eurjchem-1783	253	38	1h	1h	NUM
eurjchem-1783	253	39	,	,	PUNCT
eurjchem-1783	253	40	ar	ar	NOUN
eurjchem-1783	253	41	-	-	NOUN
eurjchem-1783	253	42	h	h	NOUN
eurjchem-1783	253	43	)	)	PUNCT
eurjchem-1783	253	44	,	,	PUNCT
eurjchem-1783	253	45	6.93	6.93	NUM
eurjchem-1783	253	46	(	(	PUNCT
eurjchem-1783	253	47	t	t	PROPN
eurjchem-1783	253	48	,	,	PUNCT
eurjchem-1783	253	49	j	j	PROPN
eurjchem-1783	254	1	=	=	PROPN
eurjchem-1783	254	2	9.12	9.12	NUM
eurjchem-1783	254	3	hz	hz	NOUN
eurjchem-1783	254	4	,	,	PUNCT
eurjchem-1783	254	5	1h	1h	NUM
eurjchem-1783	254	6	,	,	PUNCT
eurjchem-1783	254	7	ar	ar	NOUN
eurjchem-1783	254	8	-	-	NOUN
eurjchem-1783	254	9	h	h	NOUN
eurjchem-1783	254	10	)	)	PUNCT
eurjchem-1783	254	11	,	,	PUNCT
eurjchem-1783	254	12	4.80	4.80	NUM
eurjchem-1783	254	13	(	(	PUNCT
eurjchem-1783	254	14	m	m	PROPN
eurjchem-1783	254	15	,	,	PUNCT
eurjchem-1783	254	16	1h	1h	NUM
eurjchem-1783	254	17	,	,	PUNCT
eurjchem-1783	254	18	ch	ch	NOUN
eurjchem-1783	254	19	)	)	PUNCT
eurjchem-1783	254	20	,	,	PUNCT
eurjchem-1783	254	21	4.07	4.07	NUM
eurjchem-1783	254	22	-	-	SYM
eurjchem-1783	254	23	3.83	3.83	NUM
eurjchem-1783	254	24	(	(	PUNCT
eurjchem-1783	254	25	m	m	PROPN
eurjchem-1783	254	26	,	,	PUNCT
eurjchem-1783	254	27	2h	2h	NUM
eurjchem-1783	254	28	,	,	PUNCT
eurjchem-1783	254	29	ch2	ch2	PROPN
eurjchem-1783	254	30	)	)	PUNCT
eurjchem-1783	254	31	,	,	PUNCT
eurjchem-1783	254	32	3.83	3.83	NUM
eurjchem-1783	254	33	-	-	SYM
eurjchem-1783	254	34	3.68	3.68	NUM
eurjchem-1783	254	35	(	(	PUNCT
eurjchem-1783	254	36	m	m	PROPN
eurjchem-1783	254	37	,	,	PUNCT
eurjchem-1783	254	38	2h	2h	NUM
eurjchem-1783	254	39	,	,	PUNCT
eurjchem-1783	254	40	ch2	ch2	PROPN
eurjchem-1783	254	41	)	)	PUNCT
eurjchem-1783	254	42	,	,	PUNCT
eurjchem-1783	254	43	3.59	3.59	NUM
eurjchem-1783	254	44	(	(	PUNCT
eurjchem-1783	254	45	t	t	PROPN
eurjchem-1783	254	46	,	,	PUNCT
eurjchem-1783	254	47	j	j	PROPN
eurjchem-1783	255	1	=	=	SYM
eurjchem-1783	255	2	4.64	4.64	NUM
eurjchem-1783	255	3	hz	hz	NOUN
eurjchem-1783	255	4	,	,	PUNCT
eurjchem-1783	255	5	4h	4h	NOUN
eurjchem-1783	255	6	,	,	PUNCT
eurjchem-1783	255	7	piperazine	piperazine	NOUN
eurjchem-1783	255	8	-	-	PUNCT
eurjchem-1783	255	9	h	h	NOUN
eurjchem-1783	255	10	)	)	PUNCT
eurjchem-1783	255	11	,	,	PUNCT
eurjchem-1783	255	12	3.01	3.01	NUM
eurjchem-1783	255	13	(	(	PUNCT
eurjchem-1783	255	14	t	t	PROPN
eurjchem-1783	255	15	,	,	PUNCT
eurjchem-1783	255	16	j	j	X
eurjchem-1783	256	1	=	=	PUNCT
eurjchem-1783	256	2	4.72	4.72	NUM
eurjchem-1783	256	3	hz,4h	hz,4h	ADJ
eurjchem-1783	256	4	,	,	PUNCT
eurjchem-1783	256	5	piperazine	piperazine	NOUN
eurjchem-1783	256	6	-	-	PUNCT
eurjchem-1783	256	7	h	h	NOUN
eurjchem-1783	256	8	)	)	PUNCT
eurjchem-1783	256	9	,	,	PUNCT
eurjchem-1783	256	10	1.48	1.48	NUM
eurjchem-1783	256	11	(	(	PUNCT
eurjchem-1783	256	12	s	s	PROPN
eurjchem-1783	256	13	,	,	PUNCT
eurjchem-1783	256	14	9h	9h	NUM
eurjchem-1783	256	15	,	,	PUNCT
eurjchem-1783	256	16	boc	boc	NOUN
eurjchem-1783	256	17	-	-	NOUN
eurjchem-1783	256	18	h	h	NOUN
eurjchem-1783	256	19	)	)	PUNCT
eurjchem-1783	256	20	.	.	PUNCT
eurjchem-1783	257	1	13c	13c	NOUN
eurjchem-1783	257	2	nmr	nmr	NOUN
eurjchem-1783	257	3	(	(	PUNCT
eurjchem-1783	257	4	100	100	NUM
eurjchem-1783	257	5	mhz	mhz	NOUN
eurjchem-1783	257	6	,	,	PUNCT
eurjchem-1783	257	7	cdcl3	cdcl3	PROPN
eurjchem-1783	257	8	,	,	PUNCT
eurjchem-1783	257	9	δ	δ	PROPN
eurjchem-1783	257	10	,	,	PUNCT
eurjchem-1783	257	11	ppm	ppm	NUM
eurjchem-1783	257	12	):	):	PUNCT
eurjchem-1783	257	13	154.7	154.7	NUM
eurjchem-1783	257	14	(	(	PUNCT
eurjchem-1783	257	15	1c	1c	NOUN
eurjchem-1783	257	16	,	,	PUNCT
eurjchem-1783	257	17	co	co	NOUN
eurjchem-1783	257	18	)	)	PUNCT
eurjchem-1783	257	19	,	,	PUNCT
eurjchem-1783	257	20	154.8	154.8	NUM
eurjchem-1783	257	21	(	(	PUNCT
eurjchem-1783	257	22	1c	1c	NOUN
eurjchem-1783	257	23	,	,	PUNCT
eurjchem-1783	257	24	co	co	NOUN
eurjchem-1783	257	25	)	)	PUNCT
eurjchem-1783	257	26	,	,	PUNCT
eurjchem-1783	257	27	145.1	145.1	NUM
eurjchem-1783	257	28	(	(	PUNCT
eurjchem-1783	257	29	1c	1c	NOUN
eurjchem-1783	257	30	,	,	PUNCT
eurjchem-1783	257	31	ar	ar	NOUN
eurjchem-1783	257	32	-	-	NOUN
eurjchem-1783	257	33	c	c	NOUN
eurjchem-1783	257	34	)	)	PUNCT
eurjchem-1783	257	35	,	,	PUNCT
eurjchem-1783	257	36	133.7	133.7	NUM
eurjchem-1783	257	37	(	(	PUNCT
eurjchem-1783	257	38	1c	1c	NOUN
eurjchem-1783	257	39	,	,	PUNCT
eurjchem-1783	257	40	ar	ar	NOUN
eurjchem-1783	257	41	-	-	NOUN
eurjchem-1783	257	42	c	c	NOUN
eurjchem-1783	257	43	)	)	PUNCT
eurjchem-1783	257	44	,	,	PUNCT
eurjchem-1783	257	45	129.2	129.2	NUM
eurjchem-1783	257	46	(	(	PUNCT
eurjchem-1783	257	47	1c	1c	NOUN
eurjchem-1783	257	48	,	,	PUNCT
eurjchem-1783	257	49	ar	ar	NOUN
eurjchem-1783	257	50	-	-	NOUN
eurjchem-1783	257	51	c),120.7	c),120.7	NOUN
eurjchem-1783	257	52	(	(	PUNCT
eurjchem-1783	257	53	2c	2c	NOUN
eurjchem-1783	257	54	,	,	PUNCT
eurjchem-1783	257	55	ar	ar	NOUN
eurjchem-1783	257	56	-	-	NOUN
eurjchem-1783	257	57	c	c	NOUN
eurjchem-1783	257	58	)	)	PUNCT
eurjchem-1783	257	59	,	,	PUNCT
eurjchem-1783	257	60	117.6	117.6	NUM
eurjchem-1783	257	61	(	(	PUNCT
eurjchem-1783	257	62	1c	1c	NOUN
eurjchem-1783	257	63	,	,	PUNCT
eurjchem-1783	257	64	ar	ar	NOUN
eurjchem-1783	257	65	-	-	NOUN
eurjchem-1783	257	66	c	c	NOUN
eurjchem-1783	257	67	)	)	PUNCT
eurjchem-1783	257	68	,	,	PUNCT
eurjchem-1783	257	69	79.8	79.8	NUM
eurjchem-1783	257	70	(	(	PUNCT
eurjchem-1783	257	71	1c	1c	NOUN
eurjchem-1783	257	72	,	,	PUNCT
eurjchem-1783	257	73	c	c	NOUN
eurjchem-1783	257	74	-	-	PUNCT
eurjchem-1783	257	75	ch3	ch3	NOUN
eurjchem-1783	257	76	)	)	PUNCT
eurjchem-1783	257	77	,	,	PUNCT
eurjchem-1783	257	78	72.9	72.9	NUM
eurjchem-1783	257	79	(	(	PUNCT
eurjchem-1783	257	80	1c	1c	NOUN
eurjchem-1783	257	81	,	,	PUNCT
eurjchem-1783	257	82	ch	ch	NOUN
eurjchem-1783	257	83	)	)	PUNCT
eurjchem-1783	257	84	,	,	PUNCT
eurjchem-1783	257	85	51.2	51.2	NUM
eurjchem-1783	257	86	(	(	PUNCT
eurjchem-1783	257	87	2c	2c	NOUN
eurjchem-1783	257	88	,	,	PUNCT
eurjchem-1783	257	89	piperazine	piperazine	NOUN
eurjchem-1783	257	90	-	-	PUNCT
eurjchem-1783	257	91	c	c	NOUN
eurjchem-1783	257	92	)	)	PUNCT
eurjchem-1783	257	93	,	,	PUNCT
eurjchem-1783	257	94	50.9	50.9	NUM
eurjchem-1783	257	95	(	(	PUNCT
eurjchem-1783	257	96	2c	2c	NOUN
eurjchem-1783	257	97	,	,	PUNCT
eurjchem-1783	257	98	piperazine	piperazine	NOUN
eurjchem-1783	257	99	-	-	PUNCT
eurjchem-1783	257	100	c	c	NOUN
eurjchem-1783	257	101	)	)	PUNCT
eurjchem-1783	257	102	,	,	PUNCT
eurjchem-1783	257	103	43.8	43.8	NUM
eurjchem-1783	257	104	(	(	PUNCT
eurjchem-1783	257	105	1c	1c	NOUN
eurjchem-1783	257	106	,	,	PUNCT
eurjchem-1783	257	107	ch2	ch2	PROPN
eurjchem-1783	257	108	)	)	PUNCT
eurjchem-1783	257	109	,	,	PUNCT
eurjchem-1783	257	110	33.8	33.8	NUM
eurjchem-1783	257	111	(	(	PUNCT
eurjchem-1783	257	112	1c	1c	NOUN
eurjchem-1783	257	113	,	,	PUNCT
eurjchem-1783	257	114	ch2br	ch2br	NOUN
eurjchem-1783	257	115	)	)	PUNCT
eurjchem-1783	257	116	,	,	PUNCT
eurjchem-1783	257	117	28.3	28.3	NUM
eurjchem-1783	257	118	(	(	PUNCT
eurjchem-1783	257	119	3c	3c	NUM
eurjchem-1783	257	120	,	,	PUNCT
eurjchem-1783	257	121	ch3	ch3	PROPN
eurjchem-1783	257	122	)	)	PUNCT
eurjchem-1783	257	123	.	.	PUNCT
eurjchem-1783	258	1	ms	ms	NOUN
eurjchem-1783	258	2	(	(	PUNCT
eurjchem-1783	258	3	m	m	PROPN
eurjchem-1783	258	4	/	/	SYM
eurjchem-1783	258	5	z	z	NOUN
eurjchem-1783	258	6	):	):	PUNCT
eurjchem-1783	258	7	458.10	458.10	NUM
eurjchem-1783	258	8	(	(	PUNCT
eurjchem-1783	258	9	m+	m+	NUM
eurjchem-1783	258	10	)	)	PUNCT
eurjchem-1783	258	11	.	.	PUNCT
eurjchem-1783	259	1	anal	anal	PROPN
eurjchem-1783	259	2	.	.	PUNCT
eurjchem-1783	259	3	calcd	calcd	NOUN
eurjchem-1783	259	4	.	.	PUNCT
eurjchem-1783	260	1	for	for	SCONJ
eurjchem-1783	260	2	c19h25brfn3o4	c19h25brfn3o4	PROPN
eurjchem-1783	260	3	:	:	PUNCT
eurjchem-1783	260	4	c	c	X
eurjchem-1783	260	5	,	,	PUNCT
eurjchem-1783	260	6	49.79	49.79	NUM
eurjchem-1783	260	7	;	;	PUNCT
eurjchem-1783	260	8	h	h	NOUN
eurjchem-1783	260	9	,	,	PUNCT
eurjchem-1783	260	10	5.50	5.50	NUM
eurjchem-1783	260	11	;	;	PUNCT
eurjchem-1783	260	12	n	n	CCONJ
eurjchem-1783	260	13	,	,	PUNCT
eurjchem-1783	260	14	9.17	9.17	NUM
eurjchem-1783	260	15	.	.	PUNCT
eurjchem-1783	260	16	found	find	VERB
eurjchem-1783	260	17	:	:	PUNCT
eurjchem-1783	261	1	c	c	X
eurjchem-1783	261	2	,	,	PUNCT
eurjchem-1783	261	3	49.65	49.65	NUM
eurjchem-1783	261	4	;	;	PUNCT
eurjchem-1783	261	5	h	h	NOUN
eurjchem-1783	261	6	,	,	PUNCT
eurjchem-1783	261	7	5.45	5.45	NUM
eurjchem-1783	261	8	;	;	PUNCT
eurjchem-1783	261	9	n	n	CCONJ
eurjchem-1783	261	10	,	,	PUNCT
eurjchem-1783	261	11	9.13	9.13	NUM
eurjchem-1783	261	12	%	%	NOUN
eurjchem-1783	261	13	.	.	PUNCT
eurjchem-1783	262	1	2.2.11	2.2.11	X
eurjchem-1783	262	2	.	.	PUNCT
eurjchem-1783	263	1	synthesis	synthesis	NOUN
eurjchem-1783	263	2	of	of	ADP
eurjchem-1783	263	3	(	(	PUNCT
eurjchem-1783	263	4	s)-tert	s)-tert	NOUN
eurjchem-1783	263	5	-	-	PUNCT
eurjchem-1783	263	6	butyl	butyl	NOUN
eurjchem-1783	263	7	4-(4-(5-(acetamido	4-(4-(5-(acetamido	NOUN
eurjchem-1783	263	8	methyl)-2	methyl)-2	NOUN
eurjchem-1783	263	9	-	-	PUNCT
eurjchem-1783	263	10	oxooxazolidin-3	oxooxazolidin-3	NUM
eurjchem-1783	263	11	-	-	PUNCT
eurjchem-1783	263	12	yl)-2	yl)-2	NOUN
eurjchem-1783	263	13	-	-	PUNCT
eurjchem-1783	263	14	fluorophenyl	fluorophenyl	NOUN
eurjchem-1783	263	15	)	)	PUNCT
eurjchem-1783	263	16	piperazine1	piperazine1	NOUN
eurjchem-1783	263	17	-	-	NOUN
eurjchem-1783	263	18	carboxylate	carboxylate	NOUN
eurjchem-1783	263	19	(	(	PUNCT
eurjchem-1783	263	20	11	11	NUM
eurjchem-1783	263	21	)	)	PUNCT
eurjchem-1783	263	22	tert	tert	NOUN
eurjchem-1783	263	23	-	-	PUNCT
eurjchem-1783	263	24	butyl	butyl	NOUN
eurjchem-1783	263	25	4-(4-(5-(chloromethyl)-2	4-(4-(5-(chloromethyl)-2	NOUN
eurjchem-1783	263	26	-	-	PUNCT
eurjchem-1783	263	27	oxooxazolidin-3	oxooxazolidin-3	NUM
eurjchem-1783	263	28	-	-	PUNCT
eurjchem-1783	263	29	yl)2	yl)2	PROPN
eurjchem-1783	263	30	-	-	PUNCT
eurjchem-1783	263	31	fluorophenyl)piperazine-1	fluorophenyl)piperazine-1	NOUN
eurjchem-1783	263	32	-	-	NOUN
eurjchem-1783	263	33	carboxylate	carboxylate	NOUN
eurjchem-1783	263	34	(	(	PUNCT
eurjchem-1783	263	35	5	5	NUM
eurjchem-1783	263	36	g	g	NOUN
eurjchem-1783	263	37	,	,	PUNCT
eurjchem-1783	263	38	0.012	0.012	NUM
eurjchem-1783	263	39	mol	mol	NOUN
eurjchem-1783	263	40	)	)	PUNCT
eurjchem-1783	263	41	was	be	AUX
eurjchem-1783	263	42	dissolved	dissolve	VERB
eurjchem-1783	263	43	in	in	ADP
eurjchem-1783	263	44	dry	dry	ADJ
eurjchem-1783	263	45	acetonitrile	acetonitrile	NOUN
eurjchem-1783	263	46	(	(	PUNCT
eurjchem-1783	263	47	50	50	NUM
eurjchem-1783	263	48	ml	ml	NOUN
eurjchem-1783	263	49	)	)	PUNCT
eurjchem-1783	263	50	,	,	PUNCT
eurjchem-1783	263	51	added	add	VERB
eurjchem-1783	263	52	cesium	cesium	NOUN
eurjchem-1783	263	53	carbonate	carbonate	NOUN
eurjchem-1783	263	54	(	(	PUNCT
eurjchem-1783	263	55	5.91	5.91	NUM
eurjchem-1783	263	56	g	g	NOUN
eurjchem-1783	263	57	,	,	PUNCT
eurjchem-1783	263	58	0.018	0.018	NUM
eurjchem-1783	263	59	mol	mol	NOUN
eurjchem-1783	263	60	)	)	PUNCT
eurjchem-1783	263	61	,	,	PUNCT
eurjchem-1783	263	62	acetamide	acetamide	NOUN
eurjchem-1783	263	63	(	(	PUNCT
eurjchem-1783	263	64	0.71	0.71	NUM
eurjchem-1783	263	65	g	g	NOUN
eurjchem-1783	263	66	,	,	PUNCT
eurjchem-1783	263	67	0.013	0.013	NUM
eurjchem-1783	263	68	mol	mol	NOUN
eurjchem-1783	263	69	)	)	PUNCT
eurjchem-1783	263	70	and	and	CCONJ
eurjchem-1783	263	71	sodium	sodium	NOUN
eurjchem-1783	263	72	iodide	iodide	NOUN
eurjchem-1783	263	73	(	(	PUNCT
eurjchem-1783	263	74	0.181	0.181	NUM
eurjchem-1783	263	75	g	g	NOUN
eurjchem-1783	263	76	,	,	PUNCT
eurjchem-1783	263	77	0.0012	0.0012	NUM
eurjchem-1783	263	78	mol	mol	NOUN
eurjchem-1783	263	79	)	)	PUNCT
eurjchem-1783	263	80	,	,	PUNCT
eurjchem-1783	263	81	stirred	stir	VERB
eurjchem-1783	263	82	at	at	ADP
eurjchem-1783	263	83	room	room	NOUN
eurjchem-1783	263	84	temperature	temperature	NOUN
eurjchem-1783	263	85	for	for	ADP
eurjchem-1783	263	86	10	10	NUM
eurjchem-1783	263	87	min	min	NOUN
eurjchem-1783	263	88	and	and	CCONJ
eurjchem-1783	263	89	refluxed	refluxe	VERB
eurjchem-1783	263	90	for	for	ADP
eurjchem-1783	263	91	10	10	NUM
eurjchem-1783	263	92	hr	hr	NOUN
eurjchem-1783	263	93	.	.	PUNCT
eurjchem-1783	264	1	reaction	reaction	NOUN
eurjchem-1783	264	2	was	be	AUX
eurjchem-1783	264	3	monitored	monitor	VERB
eurjchem-1783	264	4	by	by	ADP
eurjchem-1783	264	5	tlc	tlc	NOUN
eurjchem-1783	264	6	.	.	PUNCT
eurjchem-1783	265	1	reaction	reaction	NOUN
eurjchem-1783	265	2	mixture	mixture	NOUN
eurjchem-1783	265	3	was	be	AUX
eurjchem-1783	265	4	cooled	cool	VERB
eurjchem-1783	265	5	,	,	PUNCT
eurjchem-1783	265	6	filtered	filter	VERB
eurjchem-1783	265	7	,	,	PUNCT
eurjchem-1783	265	8	concentrated	concentrate	VERB
eurjchem-1783	265	9	to	to	PART
eurjchem-1783	265	10	obtain	obtain	VERB
eurjchem-1783	265	11	crude	crude	ADJ
eurjchem-1783	265	12	compound	compound	NOUN
eurjchem-1783	265	13	which	which	PRON
eurjchem-1783	265	14	was	be	AUX
eurjchem-1783	265	15	further	far	ADV
eurjchem-1783	265	16	purified	purify	VERB
eurjchem-1783	265	17	by	by	ADP
eurjchem-1783	265	18	flash	flash	NOUN
eurjchem-1783	265	19	column	column	NOUN
eurjchem-1783	265	20	chromatography	chromatography	NOUN
eurjchem-1783	265	21	using	use	VERB
eurjchem-1783	265	22	30	30	NUM
eurjchem-1783	265	23	-	-	SYM
eurjchem-1783	265	24	40	40	NUM
eurjchem-1783	265	25	%	%	NOUN
eurjchem-1783	265	26	ethyl	ethyl	PROPN
eurjchem-1783	265	27	acetate	acetate	NOUN
eurjchem-1783	265	28	in	in	ADP
eurjchem-1783	265	29	hexane	hexane	NOUN
eurjchem-1783	265	30	to	to	PART
eurjchem-1783	265	31	obtain	obtain	VERB
eurjchem-1783	265	32	the	the	DET
eurjchem-1783	265	33	product	product	NOUN
eurjchem-1783	265	34	as	as	ADP
eurjchem-1783	265	35	pale	pale	ADJ
eurjchem-1783	265	36	yellow	yellow	ADJ
eurjchem-1783	265	37	color	color	NOUN
eurjchem-1783	265	38	solid	solid	ADJ
eurjchem-1783	265	39	(	(	PUNCT
eurjchem-1783	265	40	scheme	scheme	NOUN
eurjchem-1783	265	41	3	3	NUM
eurjchem-1783	265	42	)	)	PUNCT
eurjchem-1783	265	43	.	.	PUNCT
eurjchem-1783	266	1	color	color	NOUN
eurjchem-1783	266	2	:	:	PUNCT
eurjchem-1783	266	3	pale	pale	ADJ
eurjchem-1783	266	4	yellow	yellow	ADJ
eurjchem-1783	266	5	.	.	PUNCT
eurjchem-1783	267	1	yield	yield	NOUN
eurjchem-1783	267	2	:	:	PUNCT
eurjchem-1783	267	3	95	95	NUM
eurjchem-1783	267	4	%	%	NOUN
eurjchem-1783	267	5	.	.	PUNCT
eurjchem-1783	268	1	m.p	m.p	PROPN
eurjchem-1783	268	2	.	.	PROPN
eurjchem-1783	268	3	:	:	PUNCT
eurjchem-1783	269	1	211	211	NUM
eurjchem-1783	269	2	-	-	SYM
eurjchem-1783	269	3	212	212	NUM
eurjchem-1783	269	4	°	°	NOUN
eurjchem-1783	269	5	c	c	NOUN
eurjchem-1783	269	6	.	.	PUNCT
eurjchem-1783	269	7	1h	1h	NUM
eurjchem-1783	269	8	nmr	nmr	NOUN
eurjchem-1783	269	9	(	(	PUNCT
eurjchem-1783	269	10	400	400	NUM
eurjchem-1783	269	11	mhz	mhz	NOUN
eurjchem-1783	269	12	,	,	PUNCT
eurjchem-1783	269	13	cdcl3	cdcl3	PROPN
eurjchem-1783	269	14	,	,	PUNCT
eurjchem-1783	269	15	δ	δ	PROPN
eurjchem-1783	269	16	,	,	PUNCT
eurjchem-1783	269	17	ppm	ppm	NUM
eurjchem-1783	269	18	):	):	PUNCT
eurjchem-1783	269	19	7.46	7.46	NUM
eurjchem-1783	269	20	-	-	SYM
eurjchem-1783	269	21	7.41	7.41	NUM
eurjchem-1783	269	22	(	(	PUNCT
eurjchem-1783	269	23	dd	dd	PROPN
eurjchem-1783	269	24	,	,	PUNCT
eurjchem-1783	269	25	j	j	PROPN
eurjchem-1783	269	26	=	=	SYM
eurjchem-1783	269	27	14.16	14.16	NUM
eurjchem-1783	269	28	hz	hz	NOUN
eurjchem-1783	269	29	,	,	PUNCT
eurjchem-1783	269	30	1h	1h	NUM
eurjchem-1783	269	31	,	,	PUNCT
eurjchem-1783	269	32	ar	ar	NOUN
eurjchem-1783	269	33	-	-	NOUN
eurjchem-1783	269	34	h	h	NOUN
eurjchem-1783	269	35	)	)	PUNCT
eurjchem-1783	269	36	,	,	PUNCT
eurjchem-1783	269	37	7.08	7.08	NUM
eurjchem-1783	269	38	-	-	SYM
eurjchem-1783	269	39	7.05	7.05	NUM
eurjchem-1783	269	40	(	(	PUNCT
eurjchem-1783	269	41	dd	dd	PROPN
eurjchem-1783	269	42	,	,	PUNCT
eurjchem-1783	269	43	j	j	PROPN
eurjchem-1783	270	1	=	=	NOUN
eurjchem-1783	270	2	8.76	8.76	NUM
eurjchem-1783	270	3	hz	hz	NOUN
eurjchem-1783	270	4	,	,	PUNCT
eurjchem-1783	270	5	1h	1h	NUM
eurjchem-1783	270	6	,	,	PUNCT
eurjchem-1783	270	7	ar	ar	NOUN
eurjchem-1783	270	8	-	-	NOUN
eurjchem-1783	270	9	h	h	NOUN
eurjchem-1783	270	10	)	)	PUNCT
eurjchem-1783	270	11	,	,	PUNCT
eurjchem-1783	270	12	6.91	6.91	NUM
eurjchem-1783	270	13	(	(	PUNCT
eurjchem-1783	270	14	t	t	PROPN
eurjchem-1783	270	15	,	,	PUNCT
eurjchem-1783	270	16	j	j	PROPN
eurjchem-1783	270	17	=	=	PROPN
eurjchem-1783	270	18	9.12	9.12	NUM
eurjchem-1783	270	19	hz	hz	NOUN
eurjchem-1783	270	20	,	,	PUNCT
eurjchem-1783	270	21	1h	1h	NUM
eurjchem-1783	270	22	,	,	PUNCT
eurjchem-1783	270	23	ar	ar	NOUN
eurjchem-1783	270	24	-	-	NOUN
eurjchem-1783	270	25	h	h	NOUN
eurjchem-1783	270	26	)	)	PUNCT
eurjchem-1783	270	27	,	,	PUNCT
eurjchem-1783	270	28	6.20	6.20	NUM
eurjchem-1783	270	29	(	(	PUNCT
eurjchem-1783	270	30	t	t	PROPN
eurjchem-1783	270	31	,	,	PUNCT
eurjchem-1783	270	32	j	j	PROPN
eurjchem-1783	271	1	=	=	PROPN
eurjchem-1783	271	2	5.92	5.92	NUM
eurjchem-1783	271	3	hz	hz	NOUN
eurjchem-1783	271	4	,	,	PUNCT
eurjchem-1783	271	5	1h	1h	NUM
eurjchem-1783	271	6	,	,	PUNCT
eurjchem-1783	271	7	nh	nh	PROPN
eurjchem-1783	271	8	)	)	PUNCT
eurjchem-1783	271	9	,	,	PUNCT
eurjchem-1783	271	10	4.78	4.78	NUM
eurjchem-1783	271	11	-	-	SYM
eurjchem-1783	271	12	4.75	4.75	NUM
eurjchem-1783	271	13	(	(	PUNCT
eurjchem-1783	271	14	m	m	PROPN
eurjchem-1783	271	15	,	,	PUNCT
eurjchem-1783	271	16	1h	1h	NUM
eurjchem-1783	271	17	,	,	PUNCT
eurjchem-1783	271	18	ch	ch	NOUN
eurjchem-1783	271	19	)	)	PUNCT
eurjchem-1783	271	20	,	,	PUNCT
eurjchem-1783	271	21	4.073.73	4.073.73	NUM
eurjchem-1783	271	22	(	(	PUNCT
eurjchem-1783	271	23	m	m	PROPN
eurjchem-1783	271	24	,	,	PUNCT
eurjchem-1783	271	25	2h	2h	NUM
eurjchem-1783	271	26	,	,	PUNCT
eurjchem-1783	271	27	ch2	ch2	PROPN
eurjchem-1783	271	28	)	)	PUNCT
eurjchem-1783	271	29	,	,	PUNCT
eurjchem-1783	271	30	3.72	3.72	NUM
eurjchem-1783	271	31	-	-	SYM
eurjchem-1783	271	32	3.61	3.61	NUM
eurjchem-1783	271	33	(	(	PUNCT
eurjchem-1783	271	34	m	m	PROPN
eurjchem-1783	271	35	,	,	PUNCT
eurjchem-1783	271	36	2h	2h	NUM
eurjchem-1783	271	37	,	,	PUNCT
eurjchem-1783	271	38	ch2	ch2	PROPN
eurjchem-1783	271	39	)	)	PUNCT
eurjchem-1783	271	40	,	,	PUNCT
eurjchem-1783	271	41	3.60	3.60	NUM
eurjchem-1783	271	42	(	(	PUNCT
eurjchem-1783	271	43	t	t	PROPN
eurjchem-1783	271	44	,	,	PUNCT
eurjchem-1783	271	45	j	j	PROPN
eurjchem-1783	272	1	=	=	SYM
eurjchem-1783	272	2	4.6	4.6	NUM
eurjchem-1783	272	3	hz	hz	NOUN
eurjchem-1783	272	4	,	,	PUNCT
eurjchem-1783	272	5	4h	4h	NOUN
eurjchem-1783	272	6	,	,	PUNCT
eurjchem-1783	272	7	piperazine	piperazine	NOUN
eurjchem-1783	272	8	-	-	PUNCT
eurjchem-1783	272	9	h	h	NOUN
eurjchem-1783	272	10	)	)	PUNCT
eurjchem-1783	272	11	,	,	PUNCT
eurjchem-1783	272	12	3.01	3.01	NUM
eurjchem-1783	272	13	(	(	PUNCT
eurjchem-1783	272	14	t	t	PROPN
eurjchem-1783	272	15	,	,	PUNCT
eurjchem-1783	272	16	j	j	PROPN
eurjchem-1783	272	17	=	=	PROPN
eurjchem-1783	272	18	4.68	4.68	NUM
eurjchem-1783	272	19	hz	hz	NOUN
eurjchem-1783	272	20	,	,	PUNCT
eurjchem-1783	272	21	4h	4h	NOUN
eurjchem-1783	272	22	,	,	PUNCT
eurjchem-1783	272	23	piperazine	piperazine	NOUN
eurjchem-1783	272	24	-	-	PUNCT
eurjchem-1783	272	25	h	h	NOUN
eurjchem-1783	272	26	)	)	PUNCT
eurjchem-1783	272	27	,	,	PUNCT
eurjchem-1783	272	28	2.04	2.04	NUM
eurjchem-1783	272	29	(	(	PUNCT
eurjchem-1783	272	30	s	s	PROPN
eurjchem-1783	272	31	,	,	PUNCT
eurjchem-1783	272	32	3h	3h	NUM
eurjchem-1783	272	33	,	,	PUNCT
eurjchem-1783	272	34	ch3	ch3	PROPN
eurjchem-1783	272	35	)	)	PUNCT
eurjchem-1783	272	36	,	,	PUNCT
eurjchem-1783	272	37	1.48	1.48	NUM
eurjchem-1783	272	38	(	(	PUNCT
eurjchem-1783	272	39	s	s	PROPN
eurjchem-1783	272	40	,	,	PUNCT
eurjchem-1783	272	41	9h	9h	NUM
eurjchem-1783	272	42	,	,	PUNCT
eurjchem-1783	272	43	boc	boc	NOUN
eurjchem-1783	272	44	-	-	NOUN
eurjchem-1783	272	45	h	h	NOUN
eurjchem-1783	272	46	)	)	PUNCT
eurjchem-1783	272	47	.	.	PUNCT
eurjchem-1783	273	1	13c	13c	NOUN
eurjchem-1783	273	2	nmr	nmr	NOUN
eurjchem-1783	273	3	(	(	PUNCT
eurjchem-1783	273	4	100	100	NUM
eurjchem-1783	273	5	mhz	mhz	NOUN
eurjchem-1783	273	6	,	,	PUNCT
eurjchem-1783	273	7	cdcl3	cdcl3	PROPN
eurjchem-1783	273	8	,	,	PUNCT
eurjchem-1783	273	9	δ	δ	PROPN
eurjchem-1783	273	10	,	,	PUNCT
eurjchem-1783	273	11	ppm	ppm	NOUN
eurjchem-1783	273	12	):	):	PUNCT
eurjchem-1783	273	13	171.5	171.5	NUM
eurjchem-1783	273	14	(	(	PUNCT
eurjchem-1783	273	15	1c	1c	NOUN
eurjchem-1783	273	16	,	,	PUNCT
eurjchem-1783	273	17	nhco	nhco	ADJ
eurjchem-1783	273	18	)	)	PUNCT
eurjchem-1783	273	19	,	,	PUNCT
eurjchem-1783	273	20	154.8	154.8	NUM
eurjchem-1783	273	21	(	(	PUNCT
eurjchem-1783	273	22	1c	1c	NOUN
eurjchem-1783	273	23	,	,	PUNCT
eurjchem-1783	273	24	co	co	NOUN
eurjchem-1783	273	25	)	)	PUNCT
eurjchem-1783	273	26	,	,	PUNCT
eurjchem-1783	273	27	154.51	154.51	NUM
eurjchem-1783	273	28	(	(	PUNCT
eurjchem-1783	273	29	1c	1c	NOUN
eurjchem-1783	273	30	,	,	PUNCT
eurjchem-1783	273	31	co	co	NOUN
eurjchem-1783	273	32	)	)	PUNCT
eurjchem-1783	273	33	,	,	PUNCT
eurjchem-1783	273	34	145.5	145.5	NUM
eurjchem-1783	273	35	(	(	PUNCT
eurjchem-1783	273	36	1c	1c	NOUN
eurjchem-1783	273	37	,	,	PUNCT
eurjchem-1783	273	38	ar	ar	NOUN
eurjchem-1783	273	39	-	-	NOUN
eurjchem-1783	273	40	c	c	NOUN
eurjchem-1783	273	41	)	)	PUNCT
eurjchem-1783	273	42	,	,	PUNCT
eurjchem-1783	273	43	133.7	133.7	NUM
eurjchem-1783	273	44	(	(	PUNCT
eurjchem-1783	273	45	1c	1c	NOUN
eurjchem-1783	273	46	,	,	PUNCT
eurjchem-1783	273	47	ar	ar	NOUN
eurjchem-1783	273	48	-	-	NOUN
eurjchem-1783	273	49	c	c	NOUN
eurjchem-1783	273	50	)	)	PUNCT
eurjchem-1783	273	51	,	,	PUNCT
eurjchem-1783	273	52	129.4	129.4	NUM
eurjchem-1783	273	53	(	(	PUNCT
eurjchem-1783	273	54	1c	1c	NOUN
eurjchem-1783	273	55	,	,	PUNCT
eurjchem-1783	273	56	ar	ar	NOUN
eurjchem-1783	273	57	-	-	NOUN
eurjchem-1783	273	58	c	c	NOUN
eurjchem-1783	273	59	)	)	PUNCT
eurjchem-1783	273	60	,	,	PUNCT
eurjchem-1783	273	61	120.8	120.8	NUM
eurjchem-1783	273	62	(	(	PUNCT
eurjchem-1783	273	63	2c	2c	NUM
eurjchem-1783	273	64	,	,	PUNCT
eurjchem-1783	273	65	ar	ar	NOUN
eurjchem-1783	273	66	-	-	NOUN
eurjchem-1783	273	67	c),117.6	c),117.6	NOUN
eurjchem-1783	273	68	(	(	PUNCT
eurjchem-1783	273	69	1c	1c	X
eurjchem-1783	273	70	,	,	PUNCT
eurjchem-1783	273	71	ar	ar	NOUN
eurjchem-1783	273	72	-	-	NOUN
eurjchem-1783	273	73	c	c	NOUN
eurjchem-1783	273	74	)	)	PUNCT
eurjchem-1783	273	75	,	,	PUNCT
eurjchem-1783	273	76	72.0	72.0	NUM
eurjchem-1783	273	77	(	(	PUNCT
eurjchem-1783	273	78	1c	1c	X
eurjchem-1783	273	79	,	,	PUNCT
eurjchem-1783	273	80	c	c	NOUN
eurjchem-1783	273	81	-	-	PUNCT
eurjchem-1783	273	82	ch3	ch3	NOUN
eurjchem-1783	273	83	)	)	PUNCT
eurjchem-1783	273	84	,	,	PUNCT
eurjchem-1783	273	85	51.5	51.5	NUM
eurjchem-1783	273	86	(	(	PUNCT
eurjchem-1783	273	87	2c	2c	NOUN
eurjchem-1783	273	88	,	,	PUNCT
eurjchem-1783	273	89	piperazinec	piperazinec	NOUN
eurjchem-1783	273	90	)	)	PUNCT
eurjchem-1783	273	91	,	,	PUNCT
eurjchem-1783	273	92	51.2	51.2	NUM
eurjchem-1783	273	93	(	(	PUNCT
eurjchem-1783	273	94	2c	2c	NOUN
eurjchem-1783	273	95	,	,	PUNCT
eurjchem-1783	273	96	piperazine	piperazine	NOUN
eurjchem-1783	273	97	-	-	PUNCT
eurjchem-1783	273	98	c	c	NOUN
eurjchem-1783	273	99	)	)	PUNCT
eurjchem-1783	273	100	,	,	PUNCT
eurjchem-1783	273	101	47.6	47.6	NUM
eurjchem-1783	273	102	(	(	PUNCT
eurjchem-1783	273	103	1c	1c	NOUN
eurjchem-1783	273	104	,	,	PUNCT
eurjchem-1783	273	105	ch2	ch2	PROPN
eurjchem-1783	273	106	)	)	PUNCT
eurjchem-1783	273	107	,	,	PUNCT
eurjchem-1783	273	108	41.8	41.8	NUM
eurjchem-1783	273	109	(	(	PUNCT
eurjchem-1783	273	110	1c	1c	NOUN
eurjchem-1783	273	111	,	,	PUNCT
eurjchem-1783	273	112	ch2	ch2	PROPN
eurjchem-1783	273	113	)	)	PUNCT
eurjchem-1783	273	114	,	,	PUNCT
eurjchem-1783	273	115	29.6	29.6	NUM
eurjchem-1783	273	116	(	(	PUNCT
eurjchem-1783	273	117	1c	1c	NOUN
eurjchem-1783	273	118	,	,	PUNCT
eurjchem-1783	273	119	c	c	NOUN
eurjchem-1783	273	120	)	)	PUNCT
eurjchem-1783	273	121	,	,	PUNCT
eurjchem-1783	273	122	28.4	28.4	NUM
eurjchem-1783	273	123	(	(	PUNCT
eurjchem-1783	273	124	3c	3c	NUM
eurjchem-1783	273	125	,	,	PUNCT
eurjchem-1783	273	126	ch3	ch3	PROPN
eurjchem-1783	273	127	)	)	PUNCT
eurjchem-1783	273	128	,	,	PUNCT
eurjchem-1783	273	129	22.9	22.9	NUM
eurjchem-1783	273	130	(	(	PUNCT
eurjchem-1783	273	131	1c	1c	X
eurjchem-1783	273	132	,	,	PUNCT
eurjchem-1783	273	133	ch3	ch3	PROPN
eurjchem-1783	273	134	)	)	PUNCT
eurjchem-1783	273	135	.	.	PUNCT
eurjchem-1783	274	1	anal	anal	PROPN
eurjchem-1783	274	2	.	.	PUNCT
eurjchem-1783	274	3	calcd	calcd	NOUN
eurjchem-1783	274	4	.	.	PUNCT
eurjchem-1783	275	1	for	for	ADP
eurjchem-1783	275	2	c21h29fn4o5	c21h29fn4o5	PROPN
eurjchem-1783	275	3	:	:	PUNCT
eurjchem-1783	275	4	c	c	X
eurjchem-1783	275	5	,	,	PUNCT
eurjchem-1783	275	6	57.79	57.79	NUM
eurjchem-1783	275	7	;	;	PUNCT
eurjchem-1783	275	8	h	h	NOUN
eurjchem-1783	275	9	,	,	PUNCT
eurjchem-1783	275	10	6.70	6.70	NUM
eurjchem-1783	275	11	;	;	PUNCT
eurjchem-1783	275	12	n	n	CCONJ
eurjchem-1783	275	13	,	,	PUNCT
eurjchem-1783	275	14	12.84	12.84	NUM
eurjchem-1783	275	15	.	.	PUNCT
eurjchem-1783	275	16	found	find	VERB
eurjchem-1783	275	17	:	:	PUNCT
eurjchem-1783	276	1	c	c	X
eurjchem-1783	276	2	,	,	PUNCT
eurjchem-1783	276	3	57.85	57.85	NUM
eurjchem-1783	276	4	;	;	PUNCT
eurjchem-1783	276	5	h	h	NOUN
eurjchem-1783	276	6	,	,	PUNCT
eurjchem-1783	276	7	6.52	6.52	NUM
eurjchem-1783	276	8	;	;	PUNCT
eurjchem-1783	276	9	n	n	CCONJ
eurjchem-1783	276	10	,	,	PUNCT
eurjchem-1783	276	11	12.86	12.86	NUM
eurjchem-1783	276	12	%	%	NOUN
eurjchem-1783	276	13	.	.	PUNCT
eurjchem-1783	277	1	2.2.12	2.2.12	X
eurjchem-1783	277	2	.	.	X
eurjchem-1783	278	1	synthesis	synthesis	NOUN
eurjchem-1783	278	2	of	of	ADP
eurjchem-1783	278	3	(	(	PUNCT
eurjchem-1783	278	4	s)-n-((3-(3	s)-n-((3-(3	PROPN
eurjchem-1783	278	5	-	-	PUNCT
eurjchem-1783	278	6	fluoro-4-(piperazin-1	fluoro-4-(piperazin-1	NOUN
eurjchem-1783	278	7	-	-	PUNCT
eurjchem-1783	278	8	yl	yl	NOUN
eurjchem-1783	278	9	)	)	PUNCT
eurjchem-1783	278	10	phenyl)-2	phenyl)-2	PROPN
eurjchem-1783	278	11	-	-	PUNCT
eurjchem-1783	278	12	oxooxazolidin-5	oxooxazolidin-5	NUM
eurjchem-1783	278	13	-	-	PUNCT
eurjchem-1783	278	14	yl	yl	NOUN
eurjchem-1783	278	15	)	)	PUNCT
eurjchem-1783	278	16	methyl	methyl	NOUN
eurjchem-1783	278	17	)	)	PUNCT
eurjchem-1783	278	18	acetamide	acetamide	NOUN
eurjchem-1783	278	19	(	(	PUNCT
eurjchem-1783	278	20	12	12	NUM
eurjchem-1783	278	21	)	)	PUNCT
eurjchem-1783	278	22	(	(	PUNCT
eurjchem-1783	278	23	s)-tert	s)-tert	NOUN
eurjchem-1783	278	24	-	-	PUNCT
eurjchem-1783	278	25	butyl	butyl	NOUN
eurjchem-1783	278	26	4-(4-(5-(acetamidomethyl)-2	4-(4-(5-(acetamidomethyl)-2	PROPN
eurjchem-1783	278	27	-	-	PUNCT
eurjchem-1783	278	28	oxooxazolidin-3	oxooxazolidin-3	NUM
eurjchem-1783	278	29	-	-	PUNCT
eurjchem-1783	278	30	yl)-2	yl)-2	NOUN
eurjchem-1783	278	31	-	-	PUNCT
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eurjchem-1783	278	33	-	-	NOUN
eurjchem-1783	278	34	carboxylate	carboxylate	NOUN
eurjchem-1783	278	35	was	be	AUX
eurjchem-1783	278	36	dissolved	dissolve	VERB
eurjchem-1783	278	37	in	in	ADP
eurjchem-1783	278	38	dichloromethane	dichloromethane	NOUN
eurjchem-1783	278	39	(	(	PUNCT
eurjchem-1783	278	40	10	10	NUM
eurjchem-1783	278	41	ml	ml	NOUN
eurjchem-1783	278	42	)	)	PUNCT
eurjchem-1783	278	43	,	,	PUNCT
eurjchem-1783	278	44	cooled	cool	VERB
eurjchem-1783	278	45	to	to	ADP
eurjchem-1783	278	46	0	0	NUM
eurjchem-1783	278	47	°	°	NOUN
eurjchem-1783	278	48	c	c	NOUN
eurjchem-1783	278	49	,	,	PUNCT
eurjchem-1783	278	50	added	add	VERB
eurjchem-1783	278	51	hcl	hcl	PROPN
eurjchem-1783	278	52	in	in	ADP
eurjchem-1783	278	53	diethyl	diethyl	NOUN
eurjchem-1783	278	54	ether	ether	NOUN
eurjchem-1783	278	55	and	and	CCONJ
eurjchem-1783	278	56	stirred	stir	VERB
eurjchem-1783	278	57	at	at	ADP
eurjchem-1783	278	58	room	room	NOUN
eurjchem-1783	278	59	temperature	temperature	NOUN
eurjchem-1783	278	60	for	for	ADP
eurjchem-1783	278	61	2	2	NUM
eurjchem-1783	278	62	hr	hr	NOUN
eurjchem-1783	278	63	.	.	PUNCT
eurjchem-1783	279	1	reaction	reaction	NOUN
eurjchem-1783	279	2	was	be	AUX
eurjchem-1783	279	3	monitored	monitor	VERB
eurjchem-1783	279	4	by	by	ADP
eurjchem-1783	279	5	tlc	tlc	PROPN
eurjchem-1783	279	6	.	.	PUNCT
eurjchem-1783	280	1	after	after	ADP
eurjchem-1783	280	2	the	the	DET
eurjchem-1783	280	3	completion	completion	NOUN
eurjchem-1783	280	4	of	of	ADP
eurjchem-1783	280	5	the	the	DET
eurjchem-1783	280	6	reaction	reaction	NOUN
eurjchem-1783	280	7	,	,	PUNCT
eurjchem-1783	280	8	reaction	reaction	NOUN
eurjchem-1783	280	9	mass	mass	NOUN
eurjchem-1783	280	10	was	be	AUX
eurjchem-1783	280	11	concentrated	concentrate	VERB
eurjchem-1783	280	12	,	,	PUNCT
eurjchem-1783	280	13	suspended	suspend	VERB
eurjchem-1783	280	14	in	in	ADP
eurjchem-1783	280	15	diethyl	diethyl	NOUN
eurjchem-1783	280	16	ether	ether	NOUN
eurjchem-1783	280	17	(	(	PUNCT
eurjchem-1783	280	18	25	25	NUM
eurjchem-1783	280	19	ml	ml	NOUN
eurjchem-1783	280	20	)	)	PUNCT
eurjchem-1783	280	21	,	,	PUNCT
eurjchem-1783	280	22	stirred	stir	VERB
eurjchem-1783	280	23	at	at	ADP
eurjchem-1783	280	24	room	room	NOUN
eurjchem-1783	280	25	temperature	temperature	NOUN
eurjchem-1783	280	26	for	for	ADP
eurjchem-1783	280	27	10	10	NUM
eurjchem-1783	280	28	minutes	minute	NOUN
eurjchem-1783	280	29	,	,	PUNCT
eurjchem-1783	280	30	filtered	filter	VERB
eurjchem-1783	280	31	and	and	CCONJ
eurjchem-1783	280	32	dried	dry	VERB
eurjchem-1783	280	33	under	under	ADP
eurjchem-1783	280	34	vacuum	vacuum	NOUN
eurjchem-1783	280	35	to	to	PART
eurjchem-1783	280	36	get	get	VERB
eurjchem-1783	280	37	the	the	DET
eurjchem-1783	280	38	pure	pure	ADJ
eurjchem-1783	280	39	product	product	NOUN
eurjchem-1783	280	40	as	as	ADP
eurjchem-1783	280	41	white	white	X
eurjchem-1783	280	42	solid	solid	ADJ
eurjchem-1783	280	43	(	(	PUNCT
eurjchem-1783	280	44	scheme	scheme	NOUN
eurjchem-1783	280	45	3	3	NUM
eurjchem-1783	280	46	)	)	PUNCT
eurjchem-1783	280	47	.	.	PUNCT
eurjchem-1783	281	1	color	color	NOUN
eurjchem-1783	281	2	:	:	PUNCT
eurjchem-1783	281	3	white	white	ADJ
eurjchem-1783	281	4	.	.	PUNCT
eurjchem-1783	282	1	yield	yield	NOUN
eurjchem-1783	282	2	:	:	PUNCT
eurjchem-1783	282	3	95	95	NUM
eurjchem-1783	282	4	%	%	NOUN
eurjchem-1783	282	5	.	.	PUNCT
eurjchem-1783	283	1	m.p	m.p	PROPN
eurjchem-1783	283	2	.	.	PROPN
eurjchem-1783	283	3	:	:	PUNCT
eurjchem-1783	284	1	156	156	NUM
eurjchem-1783	284	2	-	-	SYM
eurjchem-1783	284	3	157	157	NUM
eurjchem-1783	284	4	°	°	NOUN
eurjchem-1783	284	5	c	c	NOUN
eurjchem-1783	284	6	.	.	PUNCT
eurjchem-1783	285	1	1h	1h	NUM
eurjchem-1783	285	2	nmr	nmr	NOUN
eurjchem-1783	285	3	(	(	PUNCT
eurjchem-1783	285	4	400	400	NUM
eurjchem-1783	285	5	mhz	mhz	NOUN
eurjchem-1783	285	6	,	,	PUNCT
eurjchem-1783	285	7	cd3od	cd3od	NOUN
eurjchem-1783	285	8	,	,	PUNCT
eurjchem-1783	285	9	δ	δ	PROPN
eurjchem-1783	285	10	,	,	PUNCT
eurjchem-1783	285	11	ppm	ppm	NOUN
eurjchem-1783	285	12	):	):	PUNCT
eurjchem-1783	285	13	7.567.52	7.567.52	NUM
eurjchem-1783	285	14	(	(	PUNCT
eurjchem-1783	285	15	dd	dd	PROPN
eurjchem-1783	285	16	,	,	PUNCT
eurjchem-1783	285	17	j	j	PROPN
eurjchem-1783	285	18	=	=	SYM
eurjchem-1783	285	19	14.4	14.4	NUM
eurjchem-1783	285	20	hz	hz	NOUN
eurjchem-1783	285	21	,	,	PUNCT
eurjchem-1783	285	22	1h	1h	NUM
eurjchem-1783	285	23	,	,	PUNCT
eurjchem-1783	285	24	ar	ar	NOUN
eurjchem-1783	285	25	-	-	NOUN
eurjchem-1783	285	26	h	h	NOUN
eurjchem-1783	285	27	)	)	PUNCT
eurjchem-1783	285	28	,	,	PUNCT
eurjchem-1783	285	29	7.23	7.23	NUM
eurjchem-1783	285	30	-	-	SYM
eurjchem-1783	285	31	7.20	7.20	NUM
eurjchem-1783	285	32	(	(	PUNCT
eurjchem-1783	285	33	m	m	PROPN
eurjchem-1783	285	34	,	,	PUNCT
eurjchem-1783	285	35	1h	1h	NUM
eurjchem-1783	285	36	,	,	PUNCT
eurjchem-1783	285	37	ar	ar	NOUN
eurjchem-1783	285	38	-	-	NOUN
eurjchem-1783	285	39	h	h	NOUN
eurjchem-1783	285	40	)	)	PUNCT
eurjchem-1783	285	41	,	,	PUNCT
eurjchem-1783	285	42	7.12	7.12	NUM
eurjchem-1783	285	43	(	(	PUNCT
eurjchem-1783	285	44	t	t	PROPN
eurjchem-1783	285	45	,	,	PUNCT
eurjchem-1783	285	46	j	j	PROPN
eurjchem-1783	285	47	=	=	PROPN
eurjchem-1783	285	48	9.08	9.08	NUM
eurjchem-1783	285	49	hz	hz	NOUN
eurjchem-1783	285	50	,	,	PUNCT
eurjchem-1783	285	51	1h	1h	NUM
eurjchem-1783	285	52	,	,	PUNCT
eurjchem-1783	285	53	ar	ar	NOUN
eurjchem-1783	285	54	-	-	NOUN
eurjchem-1783	285	55	h	h	NOUN
eurjchem-1783	285	56	)	)	PUNCT
eurjchem-1783	285	57	,	,	PUNCT
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eurjchem-1783	285	59	-	-	SYM
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eurjchem-1783	285	61	(	(	PUNCT
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eurjchem-1783	285	65	,	,	PUNCT
eurjchem-1783	285	66	ch	ch	NOUN
eurjchem-1783	285	67	)	)	PUNCT
eurjchem-1783	285	68	,	,	PUNCT
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eurjchem-1783	285	72	,	,	PUNCT
eurjchem-1783	285	73	j	j	PROPN
eurjchem-1783	286	1	=	=	SYM
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eurjchem-1783	286	4	,	,	PUNCT
eurjchem-1783	286	5	1h	1h	NUM
eurjchem-1783	286	6	,	,	PUNCT
eurjchem-1783	286	7	ch2	ch2	PROPN
eurjchem-1783	286	8	)	)	PUNCT
eurjchem-1783	286	9	,	,	PUNCT
eurjchem-1783	286	10	3.80	3.80	NUM
eurjchem-1783	286	11	-	-	SYM
eurjchem-1783	286	12	3.77	3.77	NUM
eurjchem-1783	286	13	(	(	PUNCT
eurjchem-1783	286	14	m	m	PROPN
eurjchem-1783	286	15	,	,	PUNCT
eurjchem-1783	286	16	1h	1h	NUM
eurjchem-1783	286	17	,	,	PUNCT
eurjchem-1783	286	18	ch2	ch2	PROPN
eurjchem-1783	286	19	)	)	PUNCT
eurjchem-1783	286	20	,	,	PUNCT
eurjchem-1783	286	21	3.50	3.50	NUM
eurjchem-1783	286	22	(	(	PUNCT
eurjchem-1783	286	23	d	d	PROPN
eurjchem-1783	286	24	,	,	PUNCT
eurjchem-1783	286	25	j	j	PROPN
eurjchem-1783	286	26	=	=	SYM
eurjchem-1783	286	27	5	5	NUM
eurjchem-1783	286	28	hz	hz	VERB
eurjchem-1783	286	29	,	,	PUNCT
eurjchem-1783	286	30	2h	2h	NUM
eurjchem-1783	286	31	,	,	PUNCT
eurjchem-1783	286	32	ch2	ch2	PROPN
eurjchem-1783	286	33	)	)	PUNCT
eurjchem-1783	286	34	,	,	PUNCT
eurjchem-1783	286	35	3.01	3.01	NUM
eurjchem-1783	286	36	(	(	PUNCT
eurjchem-1783	286	37	m	m	PROPN
eurjchem-1783	286	38	,	,	PUNCT
eurjchem-1783	286	39	8h	8h	NUM
eurjchem-1783	286	40	,	,	PUNCT
eurjchem-1783	286	41	piperazine	piperazine	NOUN
eurjchem-1783	286	42	-	-	PUNCT
eurjchem-1783	286	43	h	h	NOUN
eurjchem-1783	286	44	)	)	PUNCT
eurjchem-1783	286	45	,	,	PUNCT
eurjchem-1783	286	46	1.96	1.96	NUM
eurjchem-1783	286	47	(	(	PUNCT
eurjchem-1783	286	48	s	s	PROPN
eurjchem-1783	286	49	,	,	PUNCT
eurjchem-1783	286	50	3h	3h	NUM
eurjchem-1783	286	51	,	,	PUNCT
eurjchem-1783	286	52	ch3	ch3	PROPN
eurjchem-1783	286	53	)	)	PUNCT
eurjchem-1783	286	54	.	.	PUNCT
eurjchem-1783	287	1	13c	13c	NOUN
eurjchem-1783	287	2	nmr	nmr	NOUN
eurjchem-1783	287	3	(	(	PUNCT
eurjchem-1783	287	4	100	100	NUM
eurjchem-1783	287	5	mhz	mhz	NOUN
eurjchem-1783	287	6	,	,	PUNCT
eurjchem-1783	287	7	cdcl3	cdcl3	PROPN
eurjchem-1783	287	8	,	,	PUNCT
eurjchem-1783	287	9	δ	δ	PROPN
eurjchem-1783	287	10	,	,	PUNCT
eurjchem-1783	287	11	ppm	ppm	NOUN
eurjchem-1783	287	12	):	):	PUNCT
eurjchem-1783	287	13	171.5	171.5	NUM
eurjchem-1783	287	14	(	(	PUNCT
eurjchem-1783	287	15	1c	1c	NOUN
eurjchem-1783	287	16	,	,	PUNCT
eurjchem-1783	287	17	co	co	NOUN
eurjchem-1783	287	18	)	)	PUNCT
eurjchem-1783	287	19	,	,	PUNCT
eurjchem-1783	287	20	154.8	154.8	NUM
eurjchem-1783	287	21	(	(	PUNCT
eurjchem-1783	287	22	1c	1c	NOUN
eurjchem-1783	287	23	,	,	PUNCT
eurjchem-1783	287	24	co	co	NOUN
eurjchem-1783	287	25	)	)	PUNCT
eurjchem-1783	287	26	,	,	PUNCT
eurjchem-1783	287	27	154.5	154.5	NUM
eurjchem-1783	287	28	(	(	PUNCT
eurjchem-1783	287	29	1c	1c	NOUN
eurjchem-1783	287	30	,	,	PUNCT
eurjchem-1783	287	31	co	co	NOUN
eurjchem-1783	287	32	)	)	PUNCT
eurjchem-1783	287	33	,	,	PUNCT
eurjchem-1783	287	34	145.5	145.5	NUM
eurjchem-1783	287	35	(	(	PUNCT
eurjchem-1783	287	36	1c	1c	NOUN
eurjchem-1783	287	37	,	,	PUNCT
eurjchem-1783	287	38	ar	ar	NOUN
eurjchem-1783	287	39	-	-	NOUN
eurjchem-1783	287	40	c	c	NOUN
eurjchem-1783	287	41	)	)	PUNCT
eurjchem-1783	287	42	,	,	PUNCT
eurjchem-1783	287	43	133.7	133.7	NUM
eurjchem-1783	287	44	(	(	PUNCT
eurjchem-1783	287	45	1c	1c	NOUN
eurjchem-1783	287	46	,	,	PUNCT
eurjchem-1783	287	47	ar	ar	NOUN
eurjchem-1783	287	48	-	-	NOUN
eurjchem-1783	287	49	c	c	NOUN
eurjchem-1783	287	50	)	)	PUNCT
eurjchem-1783	287	51	,	,	PUNCT
eurjchem-1783	287	52	129.4	129.4	NUM
eurjchem-1783	287	53	(	(	PUNCT
eurjchem-1783	287	54	1c	1c	NOUN
eurjchem-1783	287	55	,	,	PUNCT
eurjchem-1783	287	56	ar	ar	NOUN
eurjchem-1783	287	57	-	-	NOUN
eurjchem-1783	287	58	c	c	NOUN
eurjchem-1783	287	59	)	)	PUNCT
eurjchem-1783	287	60	,	,	PUNCT
eurjchem-1783	287	61	120.8	120.8	NUM
eurjchem-1783	287	62	(	(	PUNCT
eurjchem-1783	287	63	1c	1c	NOUN
eurjchem-1783	287	64	,	,	PUNCT
eurjchem-1783	287	65	ar	ar	NOUN
eurjchem-1783	287	66	-	-	NOUN
eurjchem-1783	287	67	c	c	NOUN
eurjchem-1783	287	68	)	)	PUNCT
eurjchem-1783	287	69	,	,	PUNCT
eurjchem-1783	287	70	117.6	117.6	NUM
eurjchem-1783	287	71	(	(	PUNCT
eurjchem-1783	287	72	1c	1c	NOUN
eurjchem-1783	287	73	,	,	PUNCT
eurjchem-1783	287	74	ar	ar	NOUN
eurjchem-1783	287	75	-	-	NOUN
eurjchem-1783	287	76	c	c	NOUN
eurjchem-1783	287	77	)	)	PUNCT
eurjchem-1783	287	78	,	,	PUNCT
eurjchem-1783	287	79	51.5	51.5	NUM
eurjchem-1783	287	80	(	(	PUNCT
eurjchem-1783	287	81	2c	2c	NOUN
eurjchem-1783	287	82	,	,	PUNCT
eurjchem-1783	287	83	piperazine	piperazine	NOUN
eurjchem-1783	287	84	-	-	PUNCT
eurjchem-1783	287	85	c	c	NOUN
eurjchem-1783	287	86	)	)	PUNCT
eurjchem-1783	287	87	,	,	PUNCT
eurjchem-1783	287	88	51.2	51.2	NUM
eurjchem-1783	287	89	(	(	PUNCT
eurjchem-1783	287	90	2c	2c	NOUN
eurjchem-1783	287	91	,	,	PUNCT
eurjchem-1783	287	92	piperazine	piperazine	NOUN
eurjchem-1783	287	93	-	-	PUNCT
eurjchem-1783	287	94	c	c	NOUN
eurjchem-1783	287	95	)	)	PUNCT
eurjchem-1783	287	96	,	,	PUNCT
eurjchem-1783	287	97	47.6	47.6	NUM
eurjchem-1783	287	98	(	(	PUNCT
eurjchem-1783	287	99	1c	1c	NOUN
eurjchem-1783	287	100	,	,	PUNCT
eurjchem-1783	287	101	ch	ch	NOUN
eurjchem-1783	287	102	)	)	PUNCT
eurjchem-1783	287	103	,	,	PUNCT
eurjchem-1783	287	104	41.8	41.8	NUM
eurjchem-1783	287	105	(	(	PUNCT
eurjchem-1783	287	106	1c	1c	NOUN
eurjchem-1783	287	107	,	,	PUNCT
eurjchem-1783	287	108	ch2	ch2	PROPN
eurjchem-1783	287	109	)	)	PUNCT
eurjchem-1783	287	110	,	,	PUNCT
eurjchem-1783	287	111	29.6	29.6	NUM
eurjchem-1783	287	112	(	(	PUNCT
eurjchem-1783	287	113	1c	1c	X
eurjchem-1783	287	114	,	,	PUNCT
eurjchem-1783	287	115	nh	nh	PROPN
eurjchem-1783	287	116	-	-	PUNCT
eurjchem-1783	287	117	ch2	ch2	NOUN
eurjchem-1783	287	118	)	)	PUNCT
eurjchem-1783	287	119	,	,	PUNCT
eurjchem-1783	287	120	22.4	22.4	NUM
eurjchem-1783	287	121	(	(	PUNCT
eurjchem-1783	287	122	1c	1c	NOUN
eurjchem-1783	287	123	,	,	PUNCT
eurjchem-1783	287	124	co	co	NOUN
eurjchem-1783	287	125	-	-	ADJ
eurjchem-1783	287	126	ch3	ch3	ADJ
eurjchem-1783	287	127	)	)	PUNCT
eurjchem-1783	287	128	.	.	PUNCT
eurjchem-1783	288	1	anal	anal	PROPN
eurjchem-1783	288	2	.	.	PUNCT
eurjchem-1783	289	1	cald	cald	PROPN
eurjchem-1783	289	2	.	.	PUNCT
eurjchem-1783	290	1	for	for	ADP
eurjchem-1783	290	2	c16h21fn4o3	c16h21fn4o3	NOUN
eurjchem-1783	290	3	:	:	PUNCT
eurjchem-1783	290	4	c	c	X
eurjchem-1783	290	5	,	,	PUNCT
eurjchem-1783	290	6	57.13	57.13	NUM
eurjchem-1783	290	7	;	;	PUNCT
eurjchem-1783	290	8	h	h	NOUN
eurjchem-1783	290	9	,	,	PUNCT
eurjchem-1783	290	10	6.29	6.29	NUM
eurjchem-1783	290	11	;	;	PUNCT
eurjchem-1783	290	12	n	n	CCONJ
eurjchem-1783	290	13	,	,	PUNCT
eurjchem-1783	290	14	16.66	16.66	NUM
eurjchem-1783	290	15	.	.	PUNCT
eurjchem-1783	290	16	found	find	VERB
eurjchem-1783	290	17	:	:	PUNCT
eurjchem-1783	291	1	c	c	X
eurjchem-1783	291	2	,	,	PUNCT
eurjchem-1783	291	3	57.21	57.21	NUM
eurjchem-1783	291	4	;	;	PUNCT
eurjchem-1783	292	1	h	h	NOUN
eurjchem-1783	292	2	,	,	PUNCT
eurjchem-1783	292	3	6.14	6.14	NUM
eurjchem-1783	292	4	;	;	PUNCT
eurjchem-1783	292	5	n	n	CCONJ
eurjchem-1783	292	6	,	,	PUNCT
eurjchem-1783	292	7	16.12	16.12	NUM
eurjchem-1783	292	8	%	%	NOUN
eurjchem-1783	292	9	.	.	PUNCT
eurjchem-1783	293	1	2.2.13	2.2.13	NUM
eurjchem-1783	293	2	.	.	PUNCT
eurjchem-1783	294	1	synthesis	synthesis	NOUN
eurjchem-1783	294	2	of	of	ADP
eurjchem-1783	294	3	(	(	PUNCT
eurjchem-1783	294	4	s)-n-((3-(3	s)-n-((3-(3	PROPN
eurjchem-1783	294	5	-	-	PUNCT
eurjchem-1783	294	6	fluoro-4-(4-(2	fluoro-4-(4-(2	NOUN
eurjchem-1783	294	7	-	-	PUNCT
eurjchem-1783	294	8	hydroxy	hydroxy	NOUN
eurjchem-1783	294	9	acetyl	acetyl	NOUN
eurjchem-1783	294	10	)	)	PUNCT
eurjchem-1783	294	11	piperazin-1	piperazin-1	PROPN
eurjchem-1783	294	12	-	-	PUNCT
eurjchem-1783	294	13	yl	yl	NOUN
eurjchem-1783	294	14	)	)	PUNCT
eurjchem-1783	294	15	phenyl)-2	phenyl)-2	PROPN
eurjchem-1783	294	16	-	-	PUNCT
eurjchem-1783	294	17	oxooxazolidin-5	oxooxazolidin-5	NUM
eurjchem-1783	294	18	-	-	PUNCT
eurjchem-1783	294	19	yl	yl	NOUN
eurjchem-1783	294	20	)	)	PUNCT
eurjchem-1783	294	21	methyl	methyl	NOUN
eurjchem-1783	294	22	)	)	PUNCT
eurjchem-1783	294	23	acetamide	acetamide	NOUN
eurjchem-1783	294	24	(	(	PUNCT
eurjchem-1783	294	25	13	13	NUM
eurjchem-1783	294	26	)	)	PUNCT
eurjchem-1783	294	27	(	(	PUNCT
eurjchem-1783	294	28	s)-n-((3-(3	s)-n-((3-(3	PROPN
eurjchem-1783	294	29	-	-	PUNCT
eurjchem-1783	294	30	fluoro-4-(piperazin-1	fluoro-4-(piperazin-1	NOUN
eurjchem-1783	294	31	-	-	PUNCT
eurjchem-1783	294	32	yl	yl	NOUN
eurjchem-1783	294	33	)	)	PUNCT
eurjchem-1783	294	34	phenyl)-2	phenyl)-2	PROPN
eurjchem-1783	294	35	-	-	PUNCT
eurjchem-1783	294	36	oxooxazolidin-5	oxooxazolidin-5	NUM
eurjchem-1783	294	37	-	-	PUNCT
eurjchem-1783	294	38	yl	yl	NOUN
eurjchem-1783	294	39	)	)	PUNCT
eurjchem-1783	294	40	methyl)acetamide	methyl)acetamide	PROPN
eurjchem-1783	294	41	(	(	PUNCT
eurjchem-1783	294	42	1	1	NUM
eurjchem-1783	294	43	g	g	NOUN
eurjchem-1783	294	44	,	,	PUNCT
eurjchem-1783	294	45	0.0029	0.0029	NUM
eurjchem-1783	294	46	mol	mol	NOUN
eurjchem-1783	294	47	)	)	PUNCT
eurjchem-1783	294	48	was	be	AUX
eurjchem-1783	294	49	suspended	suspend	VERB
eurjchem-1783	294	50	in	in	ADP
eurjchem-1783	294	51	dichloromethane	dichloromethane	NOUN
eurjchem-1783	294	52	(	(	PUNCT
eurjchem-1783	294	53	20	20	NUM
eurjchem-1783	294	54	ml	ml	NOUN
eurjchem-1783	294	55	)	)	PUNCT
eurjchem-1783	294	56	and	and	CCONJ
eurjchem-1783	294	57	cooled	cool	VERB
eurjchem-1783	294	58	to	to	ADP
eurjchem-1783	294	59	0	0	NUM
eurjchem-1783	294	60	°	°	ADP
eurjchem-1783	294	61	c	c	NOUN
eurjchem-1783	294	62	added	add	VERB
eurjchem-1783	294	63	trimethylamine	trimethylamine	NOUN
eurjchem-1783	294	64	(	(	PUNCT
eurjchem-1783	294	65	0.9030	0.9030	NUM
eurjchem-1783	294	66	ml	ml	NOUN
eurjchem-1783	294	67	,	,	PUNCT
eurjchem-1783	294	68	0.0089	0.0089	NUM
eurjchem-1783	294	69	mol	mol	NOUN
eurjchem-1783	294	70	)	)	PUNCT
eurjchem-1783	294	71	,	,	PUNCT
eurjchem-1783	294	72	1	1	NUM
eurjchem-1783	294	73	-	-	PUNCT
eurjchem-1783	294	74	hydroxybenzotriazole	hydroxybenzotriazole	NOUN
eurjchem-1783	294	75	(	(	PUNCT
eurjchem-1783	294	76	hobt)(0.040	hobt)(0.040	NOUN
eurjchem-1783	294	77	g	g	NOUN
eurjchem-1783	294	78	,	,	PUNCT
eurjchem-1783	294	79	0.0003	0.0003	NUM
eurjchem-1783	294	80	mol	mol	NOUN
eurjchem-1783	294	81	)	)	PUNCT
eurjchem-1783	294	82	,	,	PUNCT
eurjchem-1783	294	83	n	n	CCONJ
eurjchem-1783	294	84	-	-	PUNCT
eurjchem-1783	294	85	ethyl	ethyl	NOUN
eurjchem-1783	294	86	-	-	PUNCT
eurjchem-1783	294	87	n′-(3	n′-(3	PROPN
eurjchem-1783	294	88	-	-	PUNCT
eurjchem-1783	294	89	dimethylaminopropyl)carbodiimide	dimethylaminopropyl)carbodiimide	ADJ
eurjchem-1783	294	90	hydrochloride	hydrochloride	NOUN
eurjchem-1783	294	91	(	(	PUNCT
eurjchem-1783	294	92	edc.hcl	edc.hcl	X
eurjchem-1783	294	93	)	)	PUNCT
eurjchem-1783	294	94	(	(	PUNCT
eurjchem-1783	294	95	0.684	0.684	NUM
eurjchem-1783	294	96	g	g	NOUN
eurjchem-1783	294	97	,	,	PUNCT
eurjchem-1783	294	98	0.0030	0.0030	NUM
eurjchem-1783	294	99	mol	mol	NOUN
eurjchem-1783	294	100	)	)	PUNCT
eurjchem-1783	294	101	and	and	CCONJ
eurjchem-1783	294	102	hydroxy	hydroxy	ADJ
eurjchem-1783	294	103	acetic	acetic	ADJ
eurjchem-1783	294	104	acid	acid	NOUN
eurjchem-1783	294	105	(	(	PUNCT
eurjchem-1783	294	106	0.271	0.271	NUM
eurjchem-1783	294	107	g	g	NOUN
eurjchem-1783	294	108	,	,	PUNCT
eurjchem-1783	294	109	0.0035	0.0035	NUM
eurjchem-1783	294	110	mol	mol	NUM
eurjchem-1783	294	111	)	)	PUNCT
eurjchem-1783	294	112	.	.	PUNCT
eurjchem-1783	295	1	2018	2018	NUM
eurjchem-1783	295	2	–	–	PUNCT
eurjchem-1783	295	3	european	european	ADJ
eurjchem-1783	295	4	journal	journal	NOUN
eurjchem-1783	295	5	of	of	ADP
eurjchem-1783	295	6	chemistry	chemistry	NOUN
eurjchem-1783	295	7	–	–	PUNCT
eurjchem-1783	295	8	cc	cc	NOUN
eurjchem-1783	295	9	by	by	ADP
eurjchem-1783	295	10	nc	nc	PROPN
eurjchem-1783	295	11	–	–	PUNCT
eurjchem-1783	295	12	doi	doi	PROPN
eurjchem-1783	295	13	:	:	PUNCT
eurjchem-1783	295	14	10.5155	10.5155	NUM
eurjchem-1783	295	15	/	/	SYM
eurjchem-1783	295	16	eurjchem.9.4.353	eurjchem.9.4.353	PROPN
eurjchem-1783	295	17	-	-	PUNCT
eurjchem-1783	295	18	359.1783	359.1783	NUM
eurjchem-1783	295	19	358	358	NUM
eurjchem-1783	295	20	siddaraj	siddaraj	ADJ
eurjchem-1783	295	21	et	et	PROPN
eurjchem-1783	295	22	al	al	PROPN
eurjchem-1783	295	23	.	.	PUNCT
eurjchem-1783	295	24	/	/	SYM
eurjchem-1783	295	25	european	european	PROPN
eurjchem-1783	295	26	journal	journal	PROPN
eurjchem-1783	295	27	of	of	ADP
eurjchem-1783	295	28	chemistry	chemistry	NOUN
eurjchem-1783	295	29	9	9	NUM
eurjchem-1783	295	30	(	(	PUNCT
eurjchem-1783	295	31	4	4	NUM
eurjchem-1783	295	32	)	)	PUNCT
eurjchem-1783	295	33	(	(	PUNCT
eurjchem-1783	295	34	2018	2018	NUM
eurjchem-1783	295	35	)	)	PUNCT
eurjchem-1783	295	36	353	353	NUM
eurjchem-1783	295	37	-	-	SYM
eurjchem-1783	295	38	359	359	NUM
eurjchem-1783	295	39	table	table	NOUN
eurjchem-1783	295	40	1	1	NUM
eurjchem-1783	295	41	.	.	PUNCT
eurjchem-1783	295	42	reaction	reaction	NOUN
eurjchem-1783	295	43	condition	condition	NOUN
eurjchem-1783	295	44	optimization	optimization	NOUN
eurjchem-1783	295	45	for	for	ADP
eurjchem-1783	295	46	the	the	DET
eurjchem-1783	295	47	conversion	conversion	NOUN
eurjchem-1783	295	48	of	of	ADP
eurjchem-1783	295	49	compound	compound	NOUN
eurjchem-1783	295	50	3	3	NUM
eurjchem-1783	295	51	to	to	PART
eurjchem-1783	295	52	4	4	NUM
eurjchem-1783	295	53	(	(	PUNCT
eurjchem-1783	295	54	scheme	scheme	NOUN
eurjchem-1783	295	55	2	2	NUM
eurjchem-1783	295	56	)	)	PUNCT
eurjchem-1783	295	57	.	.	PUNCT
eurjchem-1783	296	1	entry	entry	NOUN
eurjchem-1783	296	2	catalyst	catalyst	NOUN
eurjchem-1783	296	3	condition	condition	NOUN
eurjchem-1783	296	4	time	time	NOUN
eurjchem-1783	296	5	yield	yield	NOUN
eurjchem-1783	296	6	(	(	PUNCT
eurjchem-1783	296	7	%	%	NOUN
eurjchem-1783	296	8	)	)	PUNCT
eurjchem-1783	296	9	*	*	PUNCT
eurjchem-1783	296	10	1	1	NUM
eurjchem-1783	296	11	nil	nil	NOUN
eurjchem-1783	296	12	(	(	PUNCT
eurjchem-1783	296	13	r)-2-(bromomethyl)oxirane	r)-2-(bromomethyl)oxirane	NOUN
eurjchem-1783	296	14	,	,	PUNCT
eurjchem-1783	296	15	na2co3	na2co3	ADJ
eurjchem-1783	296	16	,	,	PUNCT
eurjchem-1783	296	17	dry	dry	ADJ
eurjchem-1783	296	18	isopropyl	isopropyl	NOUN
eurjchem-1783	296	19	alcohol	alcohol	NOUN
eurjchem-1783	296	20	:	:	PUNCT
eurjchem-1783	296	21	water	water	NOUN
eurjchem-1783	296	22	(	(	PUNCT
eurjchem-1783	296	23	v	v	NOUN
eurjchem-1783	296	24	:	:	PUNCT
eurjchem-1783	296	25	v	v	NOUN
eurjchem-1783	296	26	)	)	PUNCT
eurjchem-1783	296	27	,	,	PUNCT
eurjchem-1783	296	28	reflux	reflux	VERB
eurjchem-1783	296	29	10	10	NUM
eurjchem-1783	296	30	hr	hr	NOUN
eurjchem-1783	296	31	48	48	NUM
eurjchem-1783	296	32	2	2	NUM
eurjchem-1783	296	33	nil	nil	NOUN
eurjchem-1783	296	34	(	(	PUNCT
eurjchem-1783	296	35	r)-2-(bromomethyl)oxirane	r)-2-(bromomethyl)oxirane	NOUN
eurjchem-1783	296	36	,	,	PUNCT
eurjchem-1783	296	37	na2co3	na2co3	ADJ
eurjchem-1783	296	38	,	,	PUNCT
eurjchem-1783	296	39	dry	dry	ADJ
eurjchem-1783	296	40	isopropyl	isopropyl	NOUN
eurjchem-1783	296	41	alcohol	alcohol	NOUN
eurjchem-1783	296	42	,	,	PUNCT
eurjchem-1783	296	43	reflux	reflux	VERB
eurjchem-1783	296	44	16	16	NUM
eurjchem-1783	296	45	hr	hr	NOUN
eurjchem-1783	296	46	65	65	NUM
eurjchem-1783	296	47	3	3	NUM
eurjchem-1783	296	48	nil	nil	NOUN
eurjchem-1783	296	49	(	(	PUNCT
eurjchem-1783	296	50	r)-2-(bromomethyl)oxirane	r)-2-(bromomethyl)oxirane	NOUN
eurjchem-1783	296	51	,	,	PUNCT
eurjchem-1783	296	52	k2co3	k2co3	ADJ
eurjchem-1783	296	53	,	,	PUNCT
eurjchem-1783	296	54	dry	dry	ADJ
eurjchem-1783	296	55	isopropyl	isopropyl	NOUN
eurjchem-1783	296	56	alcohol	alcohol	NOUN
eurjchem-1783	296	57	,	,	PUNCT
eurjchem-1783	296	58	reflux	reflux	VERB
eurjchem-1783	296	59	16	16	NUM
eurjchem-1783	296	60	hr	hr	NOUN
eurjchem-1783	296	61	72	72	NUM
eurjchem-1783	296	62	4	4	NUM
eurjchem-1783	296	63	nil	nil	NOUN
eurjchem-1783	296	64	(	(	PUNCT
eurjchem-1783	296	65	r)-2-(bromomethyl)oxirane	r)-2-(bromomethyl)oxirane	NOUN
eurjchem-1783	296	66	,	,	PUNCT
eurjchem-1783	296	67	cs2co3	cs2co3	ADJ
eurjchem-1783	296	68	,	,	PUNCT
eurjchem-1783	296	69	dry	dry	ADJ
eurjchem-1783	296	70	isopropyl	isopropyl	NOUN
eurjchem-1783	296	71	alcohol	alcohol	NOUN
eurjchem-1783	296	72	,	,	PUNCT
eurjchem-1783	296	73	reflux	reflux	NOUN
eurjchem-1783	296	74	9	9	NUM
eurjchem-1783	296	75	hr	hr	NOUN
eurjchem-1783	296	76	89	89	NUM
eurjchem-1783	296	77	5	5	NUM
eurjchem-1783	296	78	nil	nil	NOUN
eurjchem-1783	296	79	(	(	PUNCT
eurjchem-1783	296	80	r)-2-(bromomethyl)oxirane	r)-2-(bromomethyl)oxirane	NOUN
eurjchem-1783	296	81	,	,	PUNCT
eurjchem-1783	296	82	cs2co3	cs2co3	ADJ
eurjchem-1783	296	83	,	,	PUNCT
eurjchem-1783	296	84	acetonitrile	acetonitrile	NOUN
eurjchem-1783	296	85	,	,	PUNCT
eurjchem-1783	296	86	reflux	reflux	NOUN
eurjchem-1783	296	87	8	8	NUM
eurjchem-1783	296	88	hr	hr	NOUN
eurjchem-1783	296	89	91	91	NUM
eurjchem-1783	296	90	6	6	NUM
eurjchem-1783	296	91	nil	nil	NOUN
eurjchem-1783	296	92	(	(	PUNCT
eurjchem-1783	296	93	r)-2-(bromomethyl)oxirane	r)-2-(bromomethyl)oxirane	NOUN
eurjchem-1783	296	94	,	,	PUNCT
eurjchem-1783	296	95	cs2co3	cs2co3	ADJ
eurjchem-1783	296	96	,	,	PUNCT
eurjchem-1783	296	97	acetonitrile	acetonitrile	NOUN
eurjchem-1783	296	98	,	,	PUNCT
eurjchem-1783	296	99	reflux	reflux	VERB
eurjchem-1783	296	100	4.5	4.5	NUM
eurjchem-1783	296	101	hr	hr	NOUN
eurjchem-1783	296	102	96	96	NUM
eurjchem-1783	296	103	7	7	NUM
eurjchem-1783	296	104	nai	nai	X
eurjchem-1783	296	105	(	(	PUNCT
eurjchem-1783	296	106	r)-2-(bromomethyl)oxirane	r)-2-(bromomethyl)oxirane	NOUN
eurjchem-1783	296	107	,	,	PUNCT
eurjchem-1783	296	108	cs2co3	cs2co3	ADJ
eurjchem-1783	296	109	,	,	PUNCT
eurjchem-1783	296	110	acetonitrile	acetonitrile	NOUN
eurjchem-1783	296	111	,	,	PUNCT
eurjchem-1783	296	112	reflux	reflux	VERB
eurjchem-1783	296	113	4.5	4.5	NUM
eurjchem-1783	296	114	hr	hr	NOUN
eurjchem-1783	296	115	91	91	NUM
eurjchem-1783	296	116	*	*	PUNCT
eurjchem-1783	296	117	isolated	isolated	ADJ
eurjchem-1783	296	118	yield	yield	NOUN
eurjchem-1783	296	119	.	.	PUNCT
eurjchem-1783	297	1	table	table	NOUN
eurjchem-1783	297	2	2	2	NUM
eurjchem-1783	297	3	.	.	PUNCT
eurjchem-1783	298	1	reactions	reaction	NOUN
eurjchem-1783	298	2	condition	condition	NOUN
eurjchem-1783	298	3	optimization	optimization	NOUN
eurjchem-1783	298	4	for	for	ADP
eurjchem-1783	298	5	the	the	DET
eurjchem-1783	298	6	conversion	conversion	NOUN
eurjchem-1783	298	7	of	of	ADP
eurjchem-1783	298	8	compound	compound	NOUN
eurjchem-1783	298	9	10	10	NUM
eurjchem-1783	298	10	to	to	PART
eurjchem-1783	298	11	11	11	NUM
eurjchem-1783	298	12	(	(	PUNCT
eurjchem-1783	298	13	scheme	scheme	NOUN
eurjchem-1783	298	14	3	3	NUM
eurjchem-1783	298	15	)	)	PUNCT
eurjchem-1783	298	16	.	.	PUNCT
eurjchem-1783	299	1	entry	entry	NOUN
eurjchem-1783	299	2	catalyst	catalyst	NOUN
eurjchem-1783	299	3	conditions	condition	NOUN
eurjchem-1783	299	4	time	time	NOUN
eurjchem-1783	299	5	yield	yield	NOUN
eurjchem-1783	299	6	(	(	PUNCT
eurjchem-1783	299	7	%	%	INTJ
eurjchem-1783	299	8	)	)	PUNCT
eurjchem-1783	299	9	*	*	PUNCT
eurjchem-1783	299	10	1	1	NUM
eurjchem-1783	299	11	tbaf	tbaf	ADJ
eurjchem-1783	299	12	acetamide	acetamide	NOUN
eurjchem-1783	299	13	,	,	PUNCT
eurjchem-1783	299	14	na2co3	na2co3	PROPN
eurjchem-1783	299	15	,	,	PUNCT
eurjchem-1783	299	16	etanol	etanol	NOUN
eurjchem-1783	299	17	:	:	PUNCT
eurjchem-1783	299	18	water	water	NOUN
eurjchem-1783	299	19	(	(	PUNCT
eurjchem-1783	299	20	v	v	NOUN
eurjchem-1783	299	21	:	:	PUNCT
eurjchem-1783	299	22	v	v	NOUN
eurjchem-1783	299	23	)	)	PUNCT
eurjchem-1783	299	24	,	,	PUNCT
eurjchem-1783	299	25	reflux	reflux	NOUN
eurjchem-1783	299	26	24hr	24hr	ADJ
eurjchem-1783	299	27	5	5	NUM
eurjchem-1783	299	28	2	2	NUM
eurjchem-1783	299	29	nai	nai	NOUN
eurjchem-1783	299	30	acetamide	acetamide	NOUN
eurjchem-1783	299	31	,	,	PUNCT
eurjchem-1783	299	32	na2co3	na2co3	PROPN
eurjchem-1783	299	33	,	,	PUNCT
eurjchem-1783	299	34	etanol	etanol	NOUN
eurjchem-1783	299	35	:	:	PUNCT
eurjchem-1783	299	36	water	water	NOUN
eurjchem-1783	299	37	(	(	PUNCT
eurjchem-1783	299	38	v	v	NOUN
eurjchem-1783	299	39	:	:	PUNCT
eurjchem-1783	299	40	v	v	NOUN
eurjchem-1783	299	41	)	)	PUNCT
eurjchem-1783	299	42	,	,	PUNCT
eurjchem-1783	299	43	reflux	reflux	NOUN
eurjchem-1783	299	44	24hr	24hr	PROPN
eurjchem-1783	299	45	12	12	NUM
eurjchem-1783	299	46	3	3	NUM
eurjchem-1783	299	47	nai	nai	NOUN
eurjchem-1783	299	48	acetamide	acetamide	NOUN
eurjchem-1783	299	49	,	,	PUNCT
eurjchem-1783	299	50	na2co3	na2co3	PROPN
eurjchem-1783	299	51	,	,	PUNCT
eurjchem-1783	299	52	dry	dry	ADJ
eurjchem-1783	299	53	ethanol	ethanol	NOUN
eurjchem-1783	299	54	(	(	PUNCT
eurjchem-1783	299	55	20v	20v	NOUN
eurjchem-1783	299	56	)	)	PUNCT
eurjchem-1783	299	57	,	,	PUNCT
eurjchem-1783	299	58	reflux	reflux	VERB
eurjchem-1783	299	59	24	24	NUM
eurjchem-1783	299	60	hr	hr	NOUN
eurjchem-1783	299	61	10	10	NUM
eurjchem-1783	299	62	4	4	NUM
eurjchem-1783	299	63	nai	nai	NOUN
eurjchem-1783	299	64	acetamide	acetamide	NOUN
eurjchem-1783	299	65	,	,	PUNCT
eurjchem-1783	299	66	na2co3	na2co3	PROPN
eurjchem-1783	299	67	,	,	PUNCT
eurjchem-1783	299	68	dry	dry	ADJ
eurjchem-1783	299	69	dimethyl	dimethyl	NOUN
eurjchem-1783	299	70	formamide	formamide	ADV
eurjchem-1783	299	71	(	(	PUNCT
eurjchem-1783	299	72	20v	20v	NOUN
eurjchem-1783	299	73	)	)	PUNCT
eurjchem-1783	299	74	,	,	PUNCT
eurjchem-1783	299	75	reflux	reflux	NOUN
eurjchem-1783	299	76	24	24	NUM
eurjchem-1783	299	77	hr	hr	NOUN
eurjchem-1783	299	78	25	25	NUM
eurjchem-1783	299	79	5	5	NUM
eurjchem-1783	299	80	nai	nai	NOUN
eurjchem-1783	299	81	acetamide	acetamide	NOUN
eurjchem-1783	299	82	,	,	PUNCT
eurjchem-1783	299	83	na2co3	na2co3	PROPN
eurjchem-1783	299	84	,	,	PUNCT
eurjchem-1783	299	85	dry	dry	ADJ
eurjchem-1783	299	86	tetrahyhyrofuran	tetrahyhyrofuran	NOUN
eurjchem-1783	299	87	(	(	PUNCT
eurjchem-1783	299	88	20v	20v	NOUN
eurjchem-1783	299	89	)	)	PUNCT
eurjchem-1783	299	90	,	,	PUNCT
eurjchem-1783	299	91	reflux	reflux	NOUN
eurjchem-1783	299	92	24	24	NUM
eurjchem-1783	299	93	hr	hr	NOUN
eurjchem-1783	299	94	26	26	NUM
eurjchem-1783	299	95	6	6	NUM
eurjchem-1783	299	96	nai	nai	NOUN
eurjchem-1783	299	97	acetamide	acetamide	NOUN
eurjchem-1783	299	98	,	,	PUNCT
eurjchem-1783	299	99	na2co3	na2co3	PROPN
eurjchem-1783	299	100	,	,	PUNCT
eurjchem-1783	299	101	dry	dry	ADJ
eurjchem-1783	299	102	acetonitrile	acetonitrile	NOUN
eurjchem-1783	299	103	(	(	PUNCT
eurjchem-1783	299	104	20v	20v	NOUN
eurjchem-1783	299	105	)	)	PUNCT
eurjchem-1783	299	106	,	,	PUNCT
eurjchem-1783	299	107	reflux	reflux	NOUN
eurjchem-1783	299	108	24	24	NUM
eurjchem-1783	299	109	hr	hr	NOUN
eurjchem-1783	299	110	30	30	NUM
eurjchem-1783	299	111	7	7	NUM
eurjchem-1783	299	112	nai	nai	PROPN
eurjchem-1783	299	113	acetamide	acetamide	NOUN
eurjchem-1783	299	114	,	,	PUNCT
eurjchem-1783	299	115	k2co3	k2co3	ADJ
eurjchem-1783	299	116	,	,	PUNCT
eurjchem-1783	299	117	dry	dry	ADJ
eurjchem-1783	299	118	ethanol	ethanol	NOUN
eurjchem-1783	299	119	(	(	PUNCT
eurjchem-1783	299	120	20v	20v	NOUN
eurjchem-1783	299	121	)	)	PUNCT
eurjchem-1783	299	122	,	,	PUNCT
eurjchem-1783	299	123	room	room	NOUN
eurjchem-1783	299	124	temperature	temperature	NOUN
eurjchem-1783	299	125	24	24	NUM
eurjchem-1783	299	126	hr	hr	NOUN
eurjchem-1783	299	127	10	10	NUM
eurjchem-1783	299	128	8	8	NUM
eurjchem-1783	299	129	nai	nai	NOUN
eurjchem-1783	299	130	acetamide	acetamide	NOUN
eurjchem-1783	299	131	,	,	PUNCT
eurjchem-1783	299	132	k2co3	k2co3	ADJ
eurjchem-1783	299	133	,	,	PUNCT
eurjchem-1783	299	134	dry	dry	ADJ
eurjchem-1783	299	135	ethanol(20v	ethanol(20v	PRON
eurjchem-1783	299	136	)	)	PUNCT
eurjchem-1783	299	137	,	,	PUNCT
eurjchem-1783	299	138	reflux	reflux	VERB
eurjchem-1783	299	139	24	24	NUM
eurjchem-1783	299	140	hr	hr	NOUN
eurjchem-1783	299	141	35	35	NUM
eurjchem-1783	299	142	9	9	NUM
eurjchem-1783	299	143	nai	nai	NOUN
eurjchem-1783	299	144	acetamide	acetamide	NOUN
eurjchem-1783	299	145	,	,	PUNCT
eurjchem-1783	299	146	k2co3	k2co3	ADJ
eurjchem-1783	299	147	,	,	PUNCT
eurjchem-1783	299	148	dry	dry	ADJ
eurjchem-1783	299	149	dimethyl	dimethyl	NOUN
eurjchem-1783	299	150	formamide	formamide	ADV
eurjchem-1783	299	151	(	(	PUNCT
eurjchem-1783	299	152	20v	20v	NOUN
eurjchem-1783	299	153	)	)	PUNCT
eurjchem-1783	299	154	,	,	PUNCT
eurjchem-1783	299	155	room	room	NOUN
eurjchem-1783	299	156	temperature	temperature	NOUN
eurjchem-1783	299	157	24	24	NUM
eurjchem-1783	299	158	hr	hr	NOUN
eurjchem-1783	299	159	12	12	NUM
eurjchem-1783	299	160	10	10	NUM
eurjchem-1783	299	161	nai	nai	PROPN
eurjchem-1783	299	162	acetamide	acetamide	NOUN
eurjchem-1783	299	163	,	,	PUNCT
eurjchem-1783	299	164	k2co3	k2co3	ADJ
eurjchem-1783	299	165	,	,	PUNCT
eurjchem-1783	299	166	dry	dry	ADJ
eurjchem-1783	299	167	dimethyl	dimethyl	NOUN
eurjchem-1783	299	168	formamide	formamide	ADV
eurjchem-1783	299	169	(	(	PUNCT
eurjchem-1783	299	170	20v	20v	NOUN
eurjchem-1783	299	171	)	)	PUNCT
eurjchem-1783	299	172	,	,	PUNCT
eurjchem-1783	299	173	reflux	reflux	VERB
eurjchem-1783	299	174	24	24	NUM
eurjchem-1783	299	175	hr	hr	NOUN
eurjchem-1783	299	176	41	41	NUM
eurjchem-1783	299	177	11	11	NUM
eurjchem-1783	299	178	nai	nai	PROPN
eurjchem-1783	299	179	acetamide	acetamide	NOUN
eurjchem-1783	299	180	,	,	PUNCT
eurjchem-1783	299	181	k2co3	k2co3	ADJ
eurjchem-1783	299	182	,	,	PUNCT
eurjchem-1783	299	183	dry	dry	ADJ
eurjchem-1783	299	184	tetrahydrofuran(20v	tetrahydrofuran(20v	PRON
eurjchem-1783	299	185	)	)	PUNCT
eurjchem-1783	299	186	,	,	PUNCT
eurjchem-1783	299	187	room	room	NOUN
eurjchem-1783	299	188	temperature	temperature	NOUN
eurjchem-1783	299	189	24	24	NUM
eurjchem-1783	299	190	hr	hr	NOUN
eurjchem-1783	299	191	24	24	NUM
eurjchem-1783	299	192	12	12	NUM
eurjchem-1783	299	193	nai	nai	NOUN
eurjchem-1783	299	194	acetamide	acetamide	NOUN
eurjchem-1783	299	195	,	,	PUNCT
eurjchem-1783	299	196	k2co3	k2co3	ADJ
eurjchem-1783	299	197	,	,	PUNCT
eurjchem-1783	299	198	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-1783	299	199	(	(	PUNCT
eurjchem-1783	299	200	20v	20v	NOUN
eurjchem-1783	299	201	)	)	PUNCT
eurjchem-1783	299	202	,	,	PUNCT
eurjchem-1783	299	203	reflux	reflux	VERB
eurjchem-1783	299	204	24	24	NUM
eurjchem-1783	299	205	hr	hr	NOUN
eurjchem-1783	299	206	40	40	NUM
eurjchem-1783	299	207	13	13	NUM
eurjchem-1783	299	208	nai	nai	NOUN
eurjchem-1783	299	209	acetamide	acetamide	PROPN
eurjchem-1783	299	210	,	,	PUNCT
eurjchem-1783	299	211	k2co3	k2co3	ADJ
eurjchem-1783	299	212	,	,	PUNCT
eurjchem-1783	299	213	dry	dry	ADJ
eurjchem-1783	299	214	acetonitrile	acetonitrile	NOUN
eurjchem-1783	299	215	(	(	PUNCT
eurjchem-1783	299	216	20v	20v	NOUN
eurjchem-1783	299	217	)	)	PUNCT
eurjchem-1783	299	218	,	,	PUNCT
eurjchem-1783	299	219	room	room	NOUN
eurjchem-1783	299	220	temperature	temperature	NOUN
eurjchem-1783	299	221	24	24	NUM
eurjchem-1783	299	222	hr	hr	NOUN
eurjchem-1783	299	223	18	18	NUM
eurjchem-1783	299	224	14	14	NUM
eurjchem-1783	299	225	nai	nai	PROPN
eurjchem-1783	299	226	acetamide	acetamide	PROPN
eurjchem-1783	299	227	,	,	PUNCT
eurjchem-1783	299	228	k2co3	k2co3	ADJ
eurjchem-1783	299	229	,	,	PUNCT
eurjchem-1783	299	230	dry	dry	ADJ
eurjchem-1783	299	231	acetonitrile	acetonitrile	NOUN
eurjchem-1783	299	232	(	(	PUNCT
eurjchem-1783	299	233	20v	20v	NOUN
eurjchem-1783	299	234	)	)	PUNCT
eurjchem-1783	299	235	,	,	PUNCT
eurjchem-1783	299	236	reflux	reflux	VERB
eurjchem-1783	299	237	24	24	NUM
eurjchem-1783	299	238	hr	hr	NOUN
eurjchem-1783	299	239	45	45	NUM
eurjchem-1783	299	240	15	15	NUM
eurjchem-1783	299	241	nai	nai	NOUN
eurjchem-1783	299	242	acetamide	acetamide	NOUN
eurjchem-1783	299	243	,	,	PUNCT
eurjchem-1783	299	244	cs2co3	cs2co3	ADJ
eurjchem-1783	299	245	,	,	PUNCT
eurjchem-1783	299	246	dry	dry	ADJ
eurjchem-1783	299	247	ethanol	ethanol	NOUN
eurjchem-1783	299	248	(	(	PUNCT
eurjchem-1783	299	249	20v	20v	NOUN
eurjchem-1783	299	250	)	)	PUNCT
eurjchem-1783	299	251	,	,	PUNCT
eurjchem-1783	299	252	reflux	reflux	VERB
eurjchem-1783	299	253	18	18	NUM
eurjchem-1783	299	254	hr	hr	NOUN
eurjchem-1783	299	255	60	60	NUM
eurjchem-1783	299	256	16	16	NUM
eurjchem-1783	299	257	nai	nai	PROPN
eurjchem-1783	299	258	acetamide	acetamide	NOUN
eurjchem-1783	299	259	,	,	PUNCT
eurjchem-1783	299	260	cs2co3	cs2co3	PROPN
eurjchem-1783	299	261	,	,	PUNCT
eurjchem-1783	299	262	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-1783	299	263	(	(	PUNCT
eurjchem-1783	299	264	20v	20v	NOUN
eurjchem-1783	299	265	)	)	PUNCT
eurjchem-1783	299	266	,	,	PUNCT
eurjchem-1783	299	267	reflux	reflux	VERB
eurjchem-1783	299	268	18	18	NUM
eurjchem-1783	299	269	hr	hr	NOUN
eurjchem-1783	299	270	72	72	NUM
eurjchem-1783	299	271	17	17	NUM
eurjchem-1783	299	272	nai	nai	PROPN
eurjchem-1783	299	273	acetamide	acetamide	NOUN
eurjchem-1783	299	274	,	,	PUNCT
eurjchem-1783	299	275	cs2co3	cs2co3	PROPN
eurjchem-1783	299	276	,	,	PUNCT
eurjchem-1783	299	277	dry	dry	ADJ
eurjchem-1783	299	278	dimethyl	dimethyl	NOUN
eurjchem-1783	299	279	formamide	formamide	ADV
eurjchem-1783	299	280	(	(	PUNCT
eurjchem-1783	299	281	20v	20v	NOUN
eurjchem-1783	299	282	)	)	PUNCT
eurjchem-1783	299	283	,	,	PUNCT
eurjchem-1783	299	284	reflux	reflux	NOUN
eurjchem-1783	299	285	12	12	NUM
eurjchem-1783	299	286	-	-	SYM
eurjchem-1783	299	287	14	14	NUM
eurjchem-1783	299	288	hr	hr	NOUN
eurjchem-1783	299	289	95	95	NUM
eurjchem-1783	299	290	18	18	NUM
eurjchem-1783	299	291	nai	nai	NOUN
eurjchem-1783	299	292	acetamide	acetamide	NOUN
eurjchem-1783	299	293	,	,	PUNCT
eurjchem-1783	299	294	cs2co3	cs2co3	ADJ
eurjchem-1783	299	295	,	,	PUNCT
eurjchem-1783	299	296	dry	dry	ADJ
eurjchem-1783	299	297	acetonitrile	acetonitrile	NOUN
eurjchem-1783	299	298	(	(	PUNCT
eurjchem-1783	299	299	20v	20v	NOUN
eurjchem-1783	299	300	)	)	PUNCT
eurjchem-1783	299	301	,	,	PUNCT
eurjchem-1783	299	302	reflux	reflux	VERB
eurjchem-1783	299	303	10	10	NUM
eurjchem-1783	299	304	hr	hr	NOUN
eurjchem-1783	299	305	95	95	NUM
eurjchem-1783	299	306	19	19	NUM
eurjchem-1783	299	307	tbaf	tbaf	ADJ
eurjchem-1783	299	308	acetamide	acetamide	NOUN
eurjchem-1783	299	309	,	,	PUNCT
eurjchem-1783	299	310	cs2co3	cs2co3	ADJ
eurjchem-1783	299	311	,	,	PUNCT
eurjchem-1783	299	312	dry	dry	ADJ
eurjchem-1783	299	313	acetonitrile	acetonitrile	NOUN
eurjchem-1783	299	314	(	(	PUNCT
eurjchem-1783	299	315	20v	20v	NOUN
eurjchem-1783	299	316	)	)	PUNCT
eurjchem-1783	299	317	,	,	PUNCT
eurjchem-1783	299	318	reflux	reflux	VERB
eurjchem-1783	299	319	18	18	NUM
eurjchem-1783	299	320	hr	hr	NOUN
eurjchem-1783	299	321	91	91	NUM
eurjchem-1783	299	322	20	20	NUM
eurjchem-1783	299	323	tbai	tbai	NOUN
eurjchem-1783	299	324	acetamide	acetamide	NOUN
eurjchem-1783	299	325	,	,	PUNCT
eurjchem-1783	299	326	cs2co3	cs2co3	ADJ
eurjchem-1783	299	327	,	,	PUNCT
eurjchem-1783	299	328	dry	dry	ADJ
eurjchem-1783	299	329	acetonitrile	acetonitrile	NOUN
eurjchem-1783	299	330	(	(	PUNCT
eurjchem-1783	299	331	20v	20v	NOUN
eurjchem-1783	299	332	)	)	PUNCT
eurjchem-1783	299	333	,	,	PUNCT
eurjchem-1783	299	334	reflux	reflux	VERB
eurjchem-1783	299	335	10	10	NUM
eurjchem-1783	299	336	hr	hr	NOUN
eurjchem-1783	299	337	95	95	NUM
eurjchem-1783	299	338	*	*	PUNCT
eurjchem-1783	299	339	isolated	isolated	ADJ
eurjchem-1783	299	340	yield	yield	NOUN
eurjchem-1783	299	341	.	.	PUNCT
eurjchem-1783	300	1	reaction	reaction	NOUN
eurjchem-1783	300	2	mixture	mixture	NOUN
eurjchem-1783	300	3	was	be	AUX
eurjchem-1783	300	4	stirred	stir	VERB
eurjchem-1783	300	5	at	at	ADP
eurjchem-1783	300	6	room	room	NOUN
eurjchem-1783	300	7	temperature	temperature	NOUN
eurjchem-1783	300	8	for	for	ADP
eurjchem-1783	300	9	8	8	NUM
eurjchem-1783	300	10	hr	hr	NOUN
eurjchem-1783	300	11	.	.	PUNCT
eurjchem-1783	301	1	completion	completion	NOUN
eurjchem-1783	301	2	of	of	ADP
eurjchem-1783	301	3	the	the	DET
eurjchem-1783	301	4	reaction	reaction	NOUN
eurjchem-1783	301	5	was	be	AUX
eurjchem-1783	301	6	monitored	monitor	VERB
eurjchem-1783	301	7	by	by	ADP
eurjchem-1783	301	8	tlc	tlc	PROPN
eurjchem-1783	301	9	.	.	PUNCT
eurjchem-1783	302	1	after	after	ADP
eurjchem-1783	302	2	the	the	DET
eurjchem-1783	302	3	completion	completion	NOUN
eurjchem-1783	302	4	of	of	ADP
eurjchem-1783	302	5	the	the	DET
eurjchem-1783	302	6	reaction	reaction	NOUN
eurjchem-1783	302	7	,	,	PUNCT
eurjchem-1783	302	8	reaction	reaction	NOUN
eurjchem-1783	302	9	mass	mass	NOUN
eurjchem-1783	302	10	was	be	AUX
eurjchem-1783	302	11	added	add	VERB
eurjchem-1783	302	12	water	water	NOUN
eurjchem-1783	302	13	(	(	PUNCT
eurjchem-1783	302	14	20	20	NUM
eurjchem-1783	302	15	ml	ml	NOUN
eurjchem-1783	302	16	)	)	PUNCT
eurjchem-1783	302	17	,	,	PUNCT
eurjchem-1783	302	18	dichloromethane	dichloromethane	NOUN
eurjchem-1783	302	19	(	(	PUNCT
eurjchem-1783	302	20	20	20	NUM
eurjchem-1783	302	21	ml	ml	NOUN
eurjchem-1783	302	22	)	)	PUNCT
eurjchem-1783	302	23	,	,	PUNCT
eurjchem-1783	302	24	extracted	extract	VERB
eurjchem-1783	302	25	with	with	ADP
eurjchem-1783	302	26	dichloromethane	dichloromethane	NOUN
eurjchem-1783	302	27	,	,	PUNCT
eurjchem-1783	302	28	aqueous	aqueous	ADJ
eurjchem-1783	302	29	layer	layer	NOUN
eurjchem-1783	302	30	was	be	AUX
eurjchem-1783	302	31	re	re	VERB
eurjchem-1783	302	32	-	-	VERB
eurjchem-1783	302	33	extracted	extract	VERB
eurjchem-1783	302	34	with	with	ADP
eurjchem-1783	302	35	dichloromethane	dichloromethane	NOUN
eurjchem-1783	302	36	(	(	PUNCT
eurjchem-1783	302	37	2×10	2×10	NUM
eurjchem-1783	302	38	ml	ml	NOUN
eurjchem-1783	302	39	)	)	PUNCT
eurjchem-1783	302	40	,	,	PUNCT
eurjchem-1783	302	41	and	and	CCONJ
eurjchem-1783	302	42	combined	combine	VERB
eurjchem-1783	302	43	organic	organic	ADJ
eurjchem-1783	302	44	layer	layer	NOUN
eurjchem-1783	302	45	was	be	AUX
eurjchem-1783	302	46	dried	dry	VERB
eurjchem-1783	302	47	over	over	ADP
eurjchem-1783	302	48	na2so4	na2so4	NOUN
eurjchem-1783	302	49	,	,	PUNCT
eurjchem-1783	302	50	filtered	filter	VERB
eurjchem-1783	302	51	and	and	CCONJ
eurjchem-1783	302	52	concentrated	concentrate	VERB
eurjchem-1783	302	53	to	to	PART
eurjchem-1783	302	54	obtain	obtain	VERB
eurjchem-1783	302	55	the	the	DET
eurjchem-1783	302	56	crude	crude	ADJ
eurjchem-1783	302	57	product	product	NOUN
eurjchem-1783	302	58	.	.	PUNCT
eurjchem-1783	303	1	crude	crude	ADJ
eurjchem-1783	303	2	product	product	NOUN
eurjchem-1783	303	3	obtained	obtain	VERB
eurjchem-1783	303	4	was	be	AUX
eurjchem-1783	303	5	purified	purify	VERB
eurjchem-1783	303	6	by	by	ADP
eurjchem-1783	303	7	column	column	NOUN
eurjchem-1783	303	8	chromatography	chromatography	NOUN
eurjchem-1783	303	9	using	use	VERB
eurjchem-1783	303	10	20	20	NUM
eurjchem-1783	303	11	%	%	NOUN
eurjchem-1783	303	12	methanol	methanol	NOUN
eurjchem-1783	303	13	in	in	ADP
eurjchem-1783	303	14	dichloromethane	dichloromethane	NOUN
eurjchem-1783	303	15	to	to	PART
eurjchem-1783	303	16	afford	afford	VERB
eurjchem-1783	303	17	the	the	DET
eurjchem-1783	303	18	pure	pure	ADJ
eurjchem-1783	303	19	as	as	ADP
eurjchem-1783	303	20	white	white	ADJ
eurjchem-1783	303	21	solid	solid	ADJ
eurjchem-1783	303	22	compound	compound	NOUN
eurjchem-1783	303	23	(	(	PUNCT
eurjchem-1783	303	24	scheme	scheme	NOUN
eurjchem-1783	303	25	3	3	NUM
eurjchem-1783	303	26	)	)	PUNCT
eurjchem-1783	303	27	.	.	PUNCT
eurjchem-1783	304	1	color	color	NOUN
eurjchem-1783	304	2	:	:	PUNCT
eurjchem-1783	304	3	white	white	ADJ
eurjchem-1783	304	4	.	.	PUNCT
eurjchem-1783	305	1	yield	yield	NOUN
eurjchem-1783	305	2	:	:	PUNCT
eurjchem-1783	305	3	89	89	NUM
eurjchem-1783	305	4	%	%	NOUN
eurjchem-1783	305	5	.	.	PUNCT
eurjchem-1783	306	1	m.p	m.p	PROPN
eurjchem-1783	306	2	.	.	PROPN
eurjchem-1783	306	3	:	:	PUNCT
eurjchem-1783	307	1	174	174	NUM
eurjchem-1783	307	2	-	-	SYM
eurjchem-1783	307	3	175	175	NUM
eurjchem-1783	307	4	°	°	PROPN
eurjchem-1783	307	5	c	c	NOUN
eurjchem-1783	307	6	.	.	PUNCT
eurjchem-1783	308	1	1h	1h	NUM
eurjchem-1783	308	2	nmr	nmr	NOUN
eurjchem-1783	308	3	(	(	PUNCT
eurjchem-1783	308	4	400	400	NUM
eurjchem-1783	308	5	mhz	mhz	NOUN
eurjchem-1783	308	6	,	,	PUNCT
eurjchem-1783	308	7	cd3od	cd3od	NOUN
eurjchem-1783	308	8	,	,	PUNCT
eurjchem-1783	308	9	δ	δ	PROPN
eurjchem-1783	308	10	,	,	PUNCT
eurjchem-1783	308	11	ppm	ppm	NUM
eurjchem-1783	308	12	):	):	PUNCT
eurjchem-1783	308	13	7.56	7.56	NUM
eurjchem-1783	308	14	-	-	SYM
eurjchem-1783	308	15	7.52	7.52	NUM
eurjchem-1783	308	16	(	(	PUNCT
eurjchem-1783	308	17	dd	dd	PROPN
eurjchem-1783	308	18	,	,	PUNCT
eurjchem-1783	308	19	j	j	PROPN
eurjchem-1783	309	1	=	=	SYM
eurjchem-1783	309	2	14.4	14.4	NUM
eurjchem-1783	309	3	hz	hz	NOUN
eurjchem-1783	309	4	,	,	PUNCT
eurjchem-1783	309	5	1h	1h	NUM
eurjchem-1783	309	6	,	,	PUNCT
eurjchem-1783	309	7	ar	ar	NOUN
eurjchem-1783	309	8	-	-	NOUN
eurjchem-1783	309	9	h	h	NOUN
eurjchem-1783	309	10	)	)	PUNCT
eurjchem-1783	309	11	,	,	PUNCT
eurjchem-1783	309	12	7.23	7.23	NUM
eurjchem-1783	309	13	-	-	SYM
eurjchem-1783	309	14	7.20	7.20	NUM
eurjchem-1783	309	15	(	(	PUNCT
eurjchem-1783	309	16	m	m	PROPN
eurjchem-1783	309	17	,	,	PUNCT
eurjchem-1783	309	18	1h	1h	NUM
eurjchem-1783	309	19	,	,	PUNCT
eurjchem-1783	309	20	ar	ar	NOUN
eurjchem-1783	309	21	-	-	NOUN
eurjchem-1783	309	22	h	h	NOUN
eurjchem-1783	309	23	)	)	PUNCT
eurjchem-1783	309	24	,	,	PUNCT
eurjchem-1783	309	25	7.12	7.12	NUM
eurjchem-1783	309	26	(	(	PUNCT
eurjchem-1783	309	27	t	t	PROPN
eurjchem-1783	309	28	,	,	PUNCT
eurjchem-1783	309	29	j	j	PROPN
eurjchem-1783	310	1	=	=	PROPN
eurjchem-1783	310	2	9.08	9.08	NUM
eurjchem-1783	310	3	hz	hz	NOUN
eurjchem-1783	310	4	,	,	PUNCT
eurjchem-1783	310	5	1h	1h	NUM
eurjchem-1783	310	6	,	,	PUNCT
eurjchem-1783	310	7	ar	ar	NOUN
eurjchem-1783	310	8	-	-	NOUN
eurjchem-1783	310	9	h	h	NOUN
eurjchem-1783	310	10	)	)	PUNCT
eurjchem-1783	310	11	,	,	PUNCT
eurjchem-1783	310	12	4.79	4.79	NUM
eurjchem-1783	310	13	-	-	SYM
eurjchem-1783	310	14	4.75	4.75	NUM
eurjchem-1783	310	15	(	(	PUNCT
eurjchem-1783	310	16	m	m	PROPN
eurjchem-1783	310	17	,	,	PUNCT
eurjchem-1783	310	18	1h	1h	NUM
eurjchem-1783	310	19	,	,	PUNCT
eurjchem-1783	310	20	ch	ch	NOUN
eurjchem-1783	310	21	)	)	PUNCT
eurjchem-1783	310	22	,	,	PUNCT
eurjchem-1783	310	23	4.40	4.40	NUM
eurjchem-1783	310	24	(	(	PUNCT
eurjchem-1783	310	25	s	s	PROPN
eurjchem-1783	310	26	,	,	PUNCT
eurjchem-1783	310	27	2h	2h	NUM
eurjchem-1783	310	28	,	,	PUNCT
eurjchem-1783	310	29	ch2	ch2	PROPN
eurjchem-1783	310	30	)	)	PUNCT
eurjchem-1783	310	31	,	,	PUNCT
eurjchem-1783	310	32	4.11	4.11	NUM
eurjchem-1783	310	33	(	(	PUNCT
eurjchem-1783	310	34	t	t	PROPN
eurjchem-1783	310	35	,	,	PUNCT
eurjchem-1783	310	36	j	j	PROPN
eurjchem-1783	311	1	=	=	SYM
eurjchem-1783	311	2	9	9	NUM
eurjchem-1783	311	3	hz	hz	NOUN
eurjchem-1783	311	4	,	,	PUNCT
eurjchem-1783	311	5	1h	1h	NUM
eurjchem-1783	311	6	,	,	PUNCT
eurjchem-1783	311	7	ch2	ch2	PROPN
eurjchem-1783	311	8	)	)	PUNCT
eurjchem-1783	311	9	,	,	PUNCT
eurjchem-1783	311	10	3.80	3.80	NUM
eurjchem-1783	311	11	-	-	SYM
eurjchem-1783	311	12	3.77	3.77	NUM
eurjchem-1783	311	13	(	(	PUNCT
eurjchem-1783	311	14	m	m	PROPN
eurjchem-1783	311	15	,	,	PUNCT
eurjchem-1783	311	16	1h	1h	NUM
eurjchem-1783	311	17	,	,	PUNCT
eurjchem-1783	311	18	ch2	ch2	PROPN
eurjchem-1783	311	19	)	)	PUNCT
eurjchem-1783	311	20	,	,	PUNCT
eurjchem-1783	311	21	3.5	3.5	NUM
eurjchem-1783	311	22	(	(	PUNCT
eurjchem-1783	311	23	d	d	PROPN
eurjchem-1783	311	24	,	,	PUNCT
eurjchem-1783	311	25	j	j	PROPN
eurjchem-1783	311	26	=	=	SYM
eurjchem-1783	311	27	5	5	NUM
eurjchem-1783	311	28	hz	hz	VERB
eurjchem-1783	311	29	,	,	PUNCT
eurjchem-1783	311	30	2h	2h	NUM
eurjchem-1783	311	31	,	,	PUNCT
eurjchem-1783	311	32	ch2	ch2	PROPN
eurjchem-1783	311	33	)	)	PUNCT
eurjchem-1783	311	34	,	,	PUNCT
eurjchem-1783	311	35	3.01	3.01	NUM
eurjchem-1783	311	36	(	(	PUNCT
eurjchem-1783	311	37	m	m	PROPN
eurjchem-1783	311	38	,	,	PUNCT
eurjchem-1783	311	39	8h	8h	NUM
eurjchem-1783	311	40	,	,	PUNCT
eurjchem-1783	311	41	piperazine	piperazine	NOUN
eurjchem-1783	311	42	-	-	PUNCT
eurjchem-1783	311	43	h	h	NOUN
eurjchem-1783	311	44	)	)	PUNCT
eurjchem-1783	311	45	,	,	PUNCT
eurjchem-1783	311	46	1.96	1.96	NUM
eurjchem-1783	311	47	(	(	PUNCT
eurjchem-1783	311	48	s	s	PROPN
eurjchem-1783	311	49	,	,	PUNCT
eurjchem-1783	311	50	3h	3h	NUM
eurjchem-1783	311	51	,	,	PUNCT
eurjchem-1783	311	52	ch3	ch3	PROPN
eurjchem-1783	311	53	)	)	PUNCT
eurjchem-1783	311	54	.	.	PUNCT
eurjchem-1783	312	1	13c	13c	NOUN
eurjchem-1783	312	2	nmr	nmr	NOUN
eurjchem-1783	312	3	(	(	PUNCT
eurjchem-1783	312	4	100	100	NUM
eurjchem-1783	312	5	mhz	mhz	NOUN
eurjchem-1783	312	6	,	,	PUNCT
eurjchem-1783	312	7	cdcl3	cdcl3	PROPN
eurjchem-1783	312	8	,	,	PUNCT
eurjchem-1783	312	9	δ	δ	PROPN
eurjchem-1783	312	10	,	,	PUNCT
eurjchem-1783	312	11	ppm	ppm	NUM
eurjchem-1783	312	12	):	):	PUNCT
eurjchem-1783	312	13	171.0	171.0	NUM
eurjchem-1783	312	14	(	(	PUNCT
eurjchem-1783	312	15	1c	1c	NOUN
eurjchem-1783	312	16	,	,	PUNCT
eurjchem-1783	312	17	nhco	nhco	ADJ
eurjchem-1783	312	18	)	)	PUNCT
eurjchem-1783	312	19	,	,	PUNCT
eurjchem-1783	312	20	169.4	169.4	NUM
eurjchem-1783	312	21	(	(	PUNCT
eurjchem-1783	312	22	1c	1c	NOUN
eurjchem-1783	312	23	,	,	PUNCT
eurjchem-1783	312	24	co	co	NOUN
eurjchem-1783	312	25	)	)	PUNCT
eurjchem-1783	312	26	,	,	PUNCT
eurjchem-1783	312	27	154.3	154.3	NUM
eurjchem-1783	312	28	(	(	PUNCT
eurjchem-1783	312	29	1c	1c	NOUN
eurjchem-1783	312	30	,	,	PUNCT
eurjchem-1783	312	31	co	co	NOUN
eurjchem-1783	312	32	)	)	PUNCT
eurjchem-1783	312	33	,	,	PUNCT
eurjchem-1783	312	34	153.04	153.04	NUM
eurjchem-1783	312	35	(	(	PUNCT
eurjchem-1783	312	36	1c	1c	NOUN
eurjchem-1783	312	37	,	,	PUNCT
eurjchem-1783	312	38	ar	ar	NOUN
eurjchem-1783	312	39	-	-	NOUN
eurjchem-1783	312	40	c	c	NOUN
eurjchem-1783	312	41	)	)	PUNCT
eurjchem-1783	312	42	,	,	PUNCT
eurjchem-1783	312	43	147.2	147.2	NUM
eurjchem-1783	312	44	(	(	PUNCT
eurjchem-1783	312	45	1c	1c	NOUN
eurjchem-1783	312	46	,	,	PUNCT
eurjchem-1783	312	47	ar	ar	NOUN
eurjchem-1783	312	48	-	-	NOUN
eurjchem-1783	312	49	c	c	NOUN
eurjchem-1783	312	50	)	)	PUNCT
eurjchem-1783	312	51	,	,	PUNCT
eurjchem-1783	312	52	119.4	119.4	NUM
eurjchem-1783	312	53	(	(	PUNCT
eurjchem-1783	312	54	1c	1c	NOUN
eurjchem-1783	312	55	,	,	PUNCT
eurjchem-1783	312	56	ar	ar	NOUN
eurjchem-1783	312	57	-	-	NOUN
eurjchem-1783	312	58	c	c	NOUN
eurjchem-1783	312	59	)	)	PUNCT
eurjchem-1783	312	60	,	,	PUNCT
eurjchem-1783	312	61	116.2	116.2	NUM
eurjchem-1783	312	62	(	(	PUNCT
eurjchem-1783	312	63	1c	1c	NOUN
eurjchem-1783	312	64	,	,	PUNCT
eurjchem-1783	312	65	ar	ar	NOUN
eurjchem-1783	312	66	-	-	NOUN
eurjchem-1783	312	67	c	c	NOUN
eurjchem-1783	312	68	)	)	PUNCT
eurjchem-1783	312	69	,	,	PUNCT
eurjchem-1783	312	70	109.8	109.8	NUM
eurjchem-1783	312	71	(	(	PUNCT
eurjchem-1783	312	72	1c	1c	NOUN
eurjchem-1783	312	73	,	,	PUNCT
eurjchem-1783	312	74	ar	ar	NOUN
eurjchem-1783	312	75	-	-	NOUN
eurjchem-1783	312	76	c	c	NOUN
eurjchem-1783	312	77	)	)	PUNCT
eurjchem-1783	312	78	,	,	PUNCT
eurjchem-1783	312	79	105.8	105.8	NUM
eurjchem-1783	312	80	(	(	PUNCT
eurjchem-1783	312	81	1c	1c	NOUN
eurjchem-1783	312	82	,	,	PUNCT
eurjchem-1783	312	83	ar	ar	NOUN
eurjchem-1783	312	84	-	-	NOUN
eurjchem-1783	312	85	c	c	NOUN
eurjchem-1783	312	86	)	)	PUNCT
eurjchem-1783	312	87	,	,	PUNCT
eurjchem-1783	312	88	71.6	71.6	NUM
eurjchem-1783	312	89	(	(	PUNCT
eurjchem-1783	312	90	1c	1c	NOUN
eurjchem-1783	312	91	,	,	PUNCT
eurjchem-1783	312	92	ch	ch	NOUN
eurjchem-1783	312	93	)	)	PUNCT
eurjchem-1783	312	94	,	,	PUNCT
eurjchem-1783	312	95	66.2	66.2	NUM
eurjchem-1783	312	96	(	(	PUNCT
eurjchem-1783	312	97	1c	1c	NUM
eurjchem-1783	312	98	,	,	PUNCT
eurjchem-1783	312	99	ch2oh	ch2oh	NOUN
eurjchem-1783	312	100	)	)	PUNCT
eurjchem-1783	312	101	,	,	PUNCT
eurjchem-1783	312	102	49.51	49.51	NUM
eurjchem-1783	312	103	(	(	PUNCT
eurjchem-1783	312	104	2c	2c	NOUN
eurjchem-1783	312	105	,	,	PUNCT
eurjchem-1783	312	106	piperazine	piperazine	NOUN
eurjchem-1783	312	107	-	-	PUNCT
eurjchem-1783	312	108	c	c	NOUN
eurjchem-1783	312	109	)	)	PUNCT
eurjchem-1783	312	110	,	,	PUNCT
eurjchem-1783	312	111	47.6	47.6	NUM
eurjchem-1783	312	112	(	(	PUNCT
eurjchem-1783	312	113	2c	2c	NOUN
eurjchem-1783	312	114	,	,	PUNCT
eurjchem-1783	312	115	piperazine	piperazine	NOUN
eurjchem-1783	312	116	-	-	PUNCT
eurjchem-1783	312	117	c	c	NOUN
eurjchem-1783	312	118	)	)	PUNCT
eurjchem-1783	312	119	,	,	PUNCT
eurjchem-1783	312	120	41.6	41.6	NUM
eurjchem-1783	312	121	(	(	PUNCT
eurjchem-1783	312	122	1c	1c	NOUN
eurjchem-1783	312	123	,	,	PUNCT
eurjchem-1783	312	124	nch2	nch2	PROPN
eurjchem-1783	312	125	)	)	PUNCT
eurjchem-1783	312	126	,	,	PUNCT
eurjchem-1783	312	127	39.7	39.7	NUM
eurjchem-1783	312	128	(	(	PUNCT
eurjchem-1783	312	129	1c	1c	X
eurjchem-1783	312	130	,	,	PUNCT
eurjchem-1783	312	131	nh	nh	PROPN
eurjchem-1783	312	132	-	-	PUNCT
eurjchem-1783	312	133	ch2	ch2	NOUN
eurjchem-1783	312	134	)	)	PUNCT
eurjchem-1783	312	135	,	,	PUNCT
eurjchem-1783	312	136	22.43	22.43	NUM
eurjchem-1783	312	137	(	(	PUNCT
eurjchem-1783	312	138	1c	1c	NOUN
eurjchem-1783	312	139	,	,	PUNCT
eurjchem-1783	312	140	co	co	NOUN
eurjchem-1783	312	141	-	-	ADJ
eurjchem-1783	312	142	ch3	ch3	ADJ
eurjchem-1783	312	143	)	)	PUNCT
eurjchem-1783	312	144	.	.	PUNCT
eurjchem-1783	313	1	anal	anal	PROPN
eurjchem-1783	313	2	.	.	PUNCT
eurjchem-1783	313	3	calcd	calcd	NOUN
eurjchem-1783	313	4	.	.	PUNCT
eurjchem-1783	314	1	for	for	SCONJ
eurjchem-1783	314	2	c18h23fn4o5	c18h23fn4o5	NOUN
eurjchem-1783	314	3	:	:	PUNCT
eurjchem-1783	314	4	c	c	X
eurjchem-1783	314	5	,	,	PUNCT
eurjchem-1783	314	6	54.82	54.82	NUM
eurjchem-1783	314	7	;	;	PUNCT
eurjchem-1783	314	8	h	h	NOUN
eurjchem-1783	314	9	,	,	PUNCT
eurjchem-1783	314	10	5.88	5.88	NUM
eurjchem-1783	314	11	;	;	PUNCT
eurjchem-1783	314	12	n	n	CCONJ
eurjchem-1783	314	13	,	,	PUNCT
eurjchem-1783	314	14	14.21	14.21	NUM
eurjchem-1783	314	15	.	.	PUNCT
eurjchem-1783	314	16	found	find	VERB
eurjchem-1783	314	17	:	:	PUNCT
eurjchem-1783	315	1	c	c	X
eurjchem-1783	315	2	,	,	PUNCT
eurjchem-1783	315	3	54.68	54.68	NUM
eurjchem-1783	315	4	;	;	PUNCT
eurjchem-1783	315	5	h	h	X
eurjchem-1783	315	6	,	,	PUNCT
eurjchem-1783	315	7	5.843	5.843	NUM
eurjchem-1783	315	8	;	;	PUNCT
eurjchem-1783	315	9	n	n	CCONJ
eurjchem-1783	315	10	,	,	PUNCT
eurjchem-1783	315	11	14.32	14.32	NUM
eurjchem-1783	315	12	%	%	NOUN
eurjchem-1783	315	13	.	.	PUNCT
eurjchem-1783	316	1	3	3	X
eurjchem-1783	316	2	.	.	NOUN
eurjchem-1783	316	3	results	result	NOUN
eurjchem-1783	316	4	and	and	CCONJ
eurjchem-1783	316	5	discussion	discussion	NOUN
eurjchem-1783	316	6	in	in	ADP
eurjchem-1783	316	7	sight	sight	NOUN
eurjchem-1783	316	8	of	of	ADP
eurjchem-1783	316	9	the	the	DET
eurjchem-1783	316	10	limitations	limitation	NOUN
eurjchem-1783	316	11	associated	associate	VERB
eurjchem-1783	316	12	with	with	ADP
eurjchem-1783	316	13	the	the	DET
eurjchem-1783	316	14	previous	previous	ADJ
eurjchem-1783	316	15	synthetic	synthetic	ADJ
eurjchem-1783	316	16	methods	method	NOUN
eurjchem-1783	316	17	of	of	ADP
eurjchem-1783	316	18	linezolid	linezolid	NOUN
eurjchem-1783	316	19	and	and	CCONJ
eurjchem-1783	316	20	eperezolid	eperezolid	NOUN
eurjchem-1783	316	21	,	,	PUNCT
eurjchem-1783	316	22	herein	herein	NOUN
eurjchem-1783	316	23	we	we	PRON
eurjchem-1783	316	24	report	report	VERB
eurjchem-1783	316	25	the	the	DET
eurjchem-1783	316	26	novel	novel	ADJ
eurjchem-1783	316	27	synthetic	synthetic	ADJ
eurjchem-1783	316	28	methodology	methodology	NOUN
eurjchem-1783	316	29	.	.	PUNCT
eurjchem-1783	317	1	the	the	DET
eurjchem-1783	317	2	synthesis	synthesis	NOUN
eurjchem-1783	317	3	of	of	ADP
eurjchem-1783	317	4	linezolid	linezolid	NOUN
eurjchem-1783	317	5	and	and	CCONJ
eurjchem-1783	317	6	eperezolid	eperezolid	NOUN
eurjchem-1783	317	7	was	be	AUX
eurjchem-1783	317	8	achieved	achieve	VERB
eurjchem-1783	317	9	as	as	ADP
eurjchem-1783	317	10	per	per	ADP
eurjchem-1783	317	11	the	the	DET
eurjchem-1783	317	12	schemes	scheme	NOUN
eurjchem-1783	317	13	2	2	NUM
eurjchem-1783	317	14	and	and	CCONJ
eurjchem-1783	317	15	3	3	NUM
eurjchem-1783	317	16	.	.	NOUN
eurjchem-1783	317	17	compounds	compound	VERB
eurjchem-1783	317	18	1	1	NUM
eurjchem-1783	317	19	to	to	PART
eurjchem-1783	317	20	3	3	NUM
eurjchem-1783	317	21	in	in	ADP
eurjchem-1783	317	22	case	case	NOUN
eurjchem-1783	317	23	of	of	ADP
eurjchem-1783	317	24	linezolid	linezolid	NOUN
eurjchem-1783	317	25	and	and	CCONJ
eurjchem-1783	317	26	compounds	compound	VERB
eurjchem-1783	317	27	6	6	NUM
eurjchem-1783	317	28	to	to	PART
eurjchem-1783	317	29	9	9	NUM
eurjchem-1783	317	30	in	in	ADP
eurjchem-1783	317	31	case	case	NOUN
eurjchem-1783	317	32	of	of	ADP
eurjchem-1783	317	33	eperezolid	eperezolid	NOUN
eurjchem-1783	317	34	were	be	AUX
eurjchem-1783	317	35	obtained	obtain	VERB
eurjchem-1783	317	36	by	by	ADP
eurjchem-1783	317	37	using	use	VERB
eurjchem-1783	317	38	known	know	VERB
eurjchem-1783	317	39	methods	method	NOUN
eurjchem-1783	317	40	but	but	CCONJ
eurjchem-1783	317	41	the	the	DET
eurjchem-1783	317	42	conversation	conversation	NOUN
eurjchem-1783	317	43	of	of	ADP
eurjchem-1783	317	44	compound	compound	NOUN
eurjchem-1783	317	45	3	3	NUM
eurjchem-1783	317	46	to	to	ADP
eurjchem-1783	317	47	5	5	NUM
eurjchem-1783	317	48	and	and	CCONJ
eurjchem-1783	317	49	compound	compound	VERB
eurjchem-1783	317	50	9	9	NUM
eurjchem-1783	317	51	to	to	PART
eurjchem-1783	317	52	11	11	NUM
eurjchem-1783	317	53	were	be	AUX
eurjchem-1783	317	54	easily	easily	ADV
eurjchem-1783	317	55	achieved	achieve	VERB
eurjchem-1783	317	56	by	by	ADP
eurjchem-1783	317	57	our	our	PRON
eurjchem-1783	317	58	new	new	ADJ
eurjchem-1783	317	59	tactic	tactic	NOUN
eurjchem-1783	317	60	.	.	PUNCT
eurjchem-1783	318	1	one	one	NUM
eurjchem-1783	318	2	of	of	ADP
eurjchem-1783	318	3	the	the	DET
eurjchem-1783	318	4	key	key	ADJ
eurjchem-1783	318	5	steps	step	NOUN
eurjchem-1783	318	6	in	in	ADP
eurjchem-1783	318	7	our	our	PRON
eurjchem-1783	318	8	methodology	methodology	NOUN
eurjchem-1783	318	9	involve	involve	VERB
eurjchem-1783	318	10	the	the	DET
eurjchem-1783	318	11	conversion	conversion	NOUN
eurjchem-1783	318	12	of	of	ADP
eurjchem-1783	318	13	compound	compound	NOUN
eurjchem-1783	318	14	3	3	NUM
eurjchem-1783	318	15	to	to	ADP
eurjchem-1783	318	16	4	4	NUM
eurjchem-1783	318	17	in	in	ADP
eurjchem-1783	318	18	which	which	PRON
eurjchem-1783	318	19	best	good	ADJ
eurjchem-1783	318	20	results	result	NOUN
eurjchem-1783	318	21	was	be	AUX
eurjchem-1783	318	22	obtained	obtain	VERB
eurjchem-1783	318	23	when	when	SCONJ
eurjchem-1783	318	24	(	(	PUNCT
eurjchem-1783	318	25	r)-2-(bromomethyl)oxirane	r)-2-(bromomethyl)oxirane	NOUN
eurjchem-1783	318	26	,	,	PUNCT
eurjchem-1783	318	27	cs2co3	cs2co3	ADJ
eurjchem-1783	318	28	,	,	PUNCT
eurjchem-1783	318	29	acetonitrile	acetonitrile	NOUN
eurjchem-1783	318	30	,	,	PUNCT
eurjchem-1783	318	31	were	be	AUX
eurjchem-1783	318	32	used	use	VERB
eurjchem-1783	318	33	under	under	ADP
eurjchem-1783	318	34	reflux	reflux	NOUN
eurjchem-1783	318	35	(	(	PUNCT
eurjchem-1783	318	36	table	table	NOUN
eurjchem-1783	318	37	1	1	NUM
eurjchem-1783	318	38	,	,	PUNCT
eurjchem-1783	318	39	entry	entry	NOUN
eurjchem-1783	318	40	6	6	NUM
eurjchem-1783	318	41	)	)	PUNCT
eurjchem-1783	318	42	.	.	PUNCT
eurjchem-1783	319	1	the	the	DET
eurjchem-1783	319	2	same	same	ADJ
eurjchem-1783	319	3	method	method	NOUN
eurjchem-1783	319	4	was	be	AUX
eurjchem-1783	319	5	extended	extend	VERB
eurjchem-1783	319	6	for	for	ADP
eurjchem-1783	319	7	the	the	DET
eurjchem-1783	319	8	conversion	conversion	NOUN
eurjchem-1783	319	9	of	of	ADP
eurjchem-1783	319	10	compound	compound	NOUN
eurjchem-1783	319	11	9	9	NUM
eurjchem-1783	319	12	to	to	ADP
eurjchem-1783	319	13	10	10	NUM
eurjchem-1783	319	14	without	without	ADP
eurjchem-1783	319	15	any	any	DET
eurjchem-1783	319	16	hassle	hassle	NOUN
eurjchem-1783	319	17	since	since	SCONJ
eurjchem-1783	319	18	the	the	DET
eurjchem-1783	319	19	environment	environment	NOUN
eurjchem-1783	319	20	around	around	ADP
eurjchem-1783	319	21	the	the	DET
eurjchem-1783	319	22	functional	functional	ADJ
eurjchem-1783	319	23	groups	group	NOUN
eurjchem-1783	319	24	taking	take	VERB
eurjchem-1783	319	25	part	part	NOUN
eurjchem-1783	319	26	in	in	ADP
eurjchem-1783	319	27	the	the	DET
eurjchem-1783	319	28	reaction	reaction	NOUN
eurjchem-1783	319	29	were	be	AUX
eurjchem-1783	319	30	similar	similar	ADJ
eurjchem-1783	319	31	,	,	PUNCT
eurjchem-1783	319	32	which	which	PRON
eurjchem-1783	319	33	in	in	ADP
eurjchem-1783	319	34	turn	turn	NOUN
eurjchem-1783	319	35	proves	prove	VERB
eurjchem-1783	319	36	the	the	DET
eurjchem-1783	319	37	new	new	ADJ
eurjchem-1783	319	38	and	and	CCONJ
eurjchem-1783	319	39	easier	easy	ADJ
eurjchem-1783	319	40	way	way	NOUN
eurjchem-1783	319	41	for	for	ADP
eurjchem-1783	319	42	the	the	DET
eurjchem-1783	319	43	construction	construction	NOUN
eurjchem-1783	319	44	of	of	ADP
eurjchem-1783	319	45	(	(	PUNCT
eurjchem-1783	319	46	r)-5-(bromomethyl	r)-5-(bromomethyl	NOUN
eurjchem-1783	319	47	)	)	PUNCT
eurjchem-1783	319	48	oxazolidin-2	oxazolidin-2	NUM
eurjchem-1783	319	49	-	-	SYM
eurjchem-1783	319	50	one	one	NUM
eurjchem-1783	319	51	.	.	PUNCT
eurjchem-1783	320	1	expeditious	expeditious	ADJ
eurjchem-1783	320	2	introducetion	introducetion	NOUN
eurjchem-1783	320	3	of	of	ADP
eurjchem-1783	320	4	acetamide	acetamide	NOUN
eurjchem-1783	320	5	group	group	NOUN
eurjchem-1783	320	6	was	be	AUX
eurjchem-1783	320	7	achieved	achieve	VERB
eurjchem-1783	320	8	by	by	ADP
eurjchem-1783	320	9	using	use	VERB
eurjchem-1783	320	10	acetamide	acetamide	NOUN
eurjchem-1783	320	11	,	,	PUNCT
eurjchem-1783	320	12	csco3	csco3	ADJ
eurjchem-1783	320	13	with	with	ADP
eurjchem-1783	320	14	catalytic	catalytic	ADJ
eurjchem-1783	320	15	amount	amount	NOUN
eurjchem-1783	320	16	of	of	ADP
eurjchem-1783	320	17	sodium	sodium	NOUN
eurjchem-1783	320	18	iodide	iodide	NOUN
eurjchem-1783	320	19	for	for	ADP
eurjchem-1783	320	20	both	both	CCONJ
eurjchem-1783	320	21	linezolid	linezolid	NOUN
eurjchem-1783	320	22	and	and	CCONJ
eurjchem-1783	320	23	eperezolid	eperezolid	NOUN
eurjchem-1783	320	24	(	(	PUNCT
eurjchem-1783	320	25	schemes	scheme	NOUN
eurjchem-1783	320	26	2	2	NUM
eurjchem-1783	320	27	and	and	CCONJ
eurjchem-1783	320	28	3	3	NUM
eurjchem-1783	320	29	)	)	PUNCT
eurjchem-1783	320	30	,	,	PUNCT
eurjchem-1783	320	31	which	which	PRON
eurjchem-1783	320	32	has	have	AUX
eurjchem-1783	320	33	indeed	indeed	ADV
eurjchem-1783	320	34	reduced	reduce	VERB
eurjchem-1783	320	35	the	the	DET
eurjchem-1783	320	36	number	number	NOUN
eurjchem-1783	320	37	of	of	ADP
eurjchem-1783	320	38	steps	step	NOUN
eurjchem-1783	320	39	involved	involve	VERB
eurjchem-1783	320	40	in	in	ADP
eurjchem-1783	320	41	the	the	DET
eurjchem-1783	320	42	overall	overall	ADJ
eurjchem-1783	320	43	synthesis	synthesis	NOUN
eurjchem-1783	320	44	.	.	PUNCT
eurjchem-1783	321	1	initially	initially	ADV
eurjchem-1783	321	2	,	,	PUNCT
eurjchem-1783	321	3	we	we	PRON
eurjchem-1783	321	4	tried	try	VERB
eurjchem-1783	321	5	the	the	DET
eurjchem-1783	321	6	reaction	reaction	NOUN
eurjchem-1783	321	7	with	with	ADP
eurjchem-1783	321	8	different	different	ADJ
eurjchem-1783	321	9	combination	combination	NOUN
eurjchem-1783	321	10	of	of	ADP
eurjchem-1783	321	11	solvents	solvent	NOUN
eurjchem-1783	321	12	and	and	CCONJ
eurjchem-1783	321	13	catalyst	catalyst	NOUN
eurjchem-1783	321	14	(	(	PUNCT
eurjchem-1783	321	15	table	table	NOUN
eurjchem-1783	321	16	2	2	NUM
eurjchem-1783	321	17	)	)	PUNCT
eurjchem-1783	321	18	,	,	PUNCT
eurjchem-1783	321	19	but	but	CCONJ
eurjchem-1783	321	20	the	the	DET
eurjchem-1783	321	21	ultimate	ultimate	ADJ
eurjchem-1783	321	22	result	result	NOUN
eurjchem-1783	321	23	was	be	AUX
eurjchem-1783	321	24	obtained	obtain	VERB
eurjchem-1783	321	25	in	in	ADP
eurjchem-1783	321	26	the	the	DET
eurjchem-1783	321	27	case	case	NOUN
eurjchem-1783	321	28	of	of	ADP
eurjchem-1783	321	29	nai	nai	PROPN
eurjchem-1783	321	30	:	:	PUNCT
eurjchem-1783	322	1	csco3	csco3	ADJ
eurjchem-1783	322	2	:	:	PUNCT
eurjchem-1783	323	1	acetonitrile	acetonitrile	NOUN
eurjchem-1783	323	2	(	(	PUNCT
eurjchem-1783	323	3	table	table	NOUN
eurjchem-1783	323	4	2	2	NUM
eurjchem-1783	323	5	,	,	PUNCT
eurjchem-1783	323	6	entry	entry	NOUN
eurjchem-1783	323	7	18	18	NUM
eurjchem-1783	323	8	)	)	PUNCT
eurjchem-1783	323	9	.	.	PUNCT
eurjchem-1783	324	1	in	in	ADP
eurjchem-1783	324	2	these	these	DET
eurjchem-1783	324	3	conditions	condition	NOUN
eurjchem-1783	324	4	,	,	PUNCT
eurjchem-1783	324	5	we	we	PRON
eurjchem-1783	324	6	achieved	achieve	VERB
eurjchem-1783	324	7	95	95	NUM
eurjchem-1783	324	8	%	%	NOUN
eurjchem-1783	324	9	of	of	ADP
eurjchem-1783	324	10	yield	yield	NOUN
eurjchem-1783	324	11	in	in	ADP
eurjchem-1783	324	12	10	10	NUM
eurjchem-1783	324	13	hr	hr	NOUN
eurjchem-1783	324	14	compared	compare	VERB
eurjchem-1783	324	15	to	to	ADP
eurjchem-1783	324	16	all	all	DET
eurjchem-1783	324	17	other	other	ADJ
eurjchem-1783	324	18	conditions	condition	NOUN
eurjchem-1783	324	19	.	.	PUNCT
eurjchem-1783	325	1	in	in	ADP
eurjchem-1783	325	2	addition	addition	NOUN
eurjchem-1783	325	3	to	to	ADP
eurjchem-1783	325	4	these	these	PRON
eurjchem-1783	325	5	in	in	ADP
eurjchem-1783	325	6	the	the	DET
eurjchem-1783	325	7	synthesis	synthesis	NOUN
eurjchem-1783	325	8	of	of	ADP
eurjchem-1783	325	9	eperezolid	eperezolid	NOUN
eurjchem-1783	325	10	,	,	PUNCT
eurjchem-1783	325	11	we	we	PRON
eurjchem-1783	325	12	have	have	AUX
eurjchem-1783	325	13	avoided	avoid	VERB
eurjchem-1783	325	14	protection	protection	NOUN
eurjchem-1783	325	15	and	and	CCONJ
eurjchem-1783	325	16	deprotection	deprotection	NOUN
eurjchem-1783	325	17	strategy	strategy	NOUN
eurjchem-1783	325	18	.	.	PUNCT
eurjchem-1783	326	1	one	one	NUM
eurjchem-1783	326	2	of	of	ADP
eurjchem-1783	326	3	the	the	DET
eurjchem-1783	326	4	early	early	ADJ
eurjchem-1783	326	5	methods	method	NOUN
eurjchem-1783	326	6	in	in	ADP
eurjchem-1783	326	7	the	the	DET
eurjchem-1783	326	8	synthesis	synthesis	NOUN
eurjchem-1783	326	9	of	of	ADP
eurjchem-1783	326	10	2	2	NUM
eurjchem-1783	326	11	-	-	PUNCT
eurjchem-1783	326	12	oxazolidinones	oxazolidinone	NOUN
eurjchem-1783	326	13	involves	involve	VERB
eurjchem-1783	326	14	the	the	DET
eurjchem-1783	326	15	reaction	reaction	NOUN
eurjchem-1783	326	16	of	of	ADP
eurjchem-1783	326	17	phosgene	phosgene	NOUN
eurjchem-1783	326	18	and	and	CCONJ
eurjchem-1783	326	19	aniline	aniline	NOUN
eurjchem-1783	326	20	with	with	ADP
eurjchem-1783	326	21	chloroethanol	chloroethanol	NOUN
eurjchem-1783	326	22	to	to	PART
eurjchem-1783	326	23	produce	produce	VERB
eurjchem-1783	326	24	chloroethyl	chloroethyl	NOUN
eurjchem-1783	326	25	-	-	PUNCT
eurjchem-1783	326	26	n	n	CCONJ
eurjchem-1783	326	27	-	-	PUNCT
eurjchem-1783	326	28	phenyl	phenyl	NOUN
eurjchem-1783	326	29	carbamate	carbamate	NOUN
eurjchem-1783	326	30	which	which	PRON
eurjchem-1783	326	31	is	be	AUX
eurjchem-1783	326	32	cyclized	cyclize	VERB
eurjchem-1783	326	33	by	by	ADP
eurjchem-1783	326	34	boiling	boil	VERB
eurjchem-1783	326	35	in	in	ADP
eurjchem-1783	326	36	potassium	potassium	NOUN
eurjchem-1783	326	37	hydroxide	hydroxide	NOUN
eurjchem-1783	326	38	solution	solution	NOUN
eurjchem-1783	326	39	.	.	PUNCT
eurjchem-1783	327	1	however	however	ADV
eurjchem-1783	327	2	,	,	PUNCT
eurjchem-1783	327	3	this	this	DET
eurjchem-1783	327	4	methodology	methodology	NOUN
eurjchem-1783	327	5	is	be	AUX
eurjchem-1783	327	6	not	not	PART
eurjchem-1783	327	7	well	well	ADV
eurjchem-1783	327	8	utilized	utilize	VERB
eurjchem-1783	327	9	in	in	ADP
eurjchem-1783	327	10	synthetic	synthetic	ADJ
eurjchem-1783	327	11	organic	organic	ADJ
eurjchem-1783	327	12	chemistry	chemistry	NOUN
eurjchem-1783	327	13	and	and	CCONJ
eurjchem-1783	327	14	drug	drug	NOUN
eurjchem-1783	327	15	discovery	discovery	NOUN
eurjchem-1783	327	16	probably	probably	ADV
eurjchem-1783	327	17	due	due	ADP
eurjchem-1783	327	18	to	to	ADP
eurjchem-1783	327	19	the	the	DET
eurjchem-1783	327	20	fear	fear	NOUN
eurjchem-1783	327	21	of	of	ADP
eurjchem-1783	327	22	low	low	ADJ
eurjchem-1783	327	23	stability	stability	NOUN
eurjchem-1783	327	24	of	of	ADP
eurjchem-1783	327	25	1	1	NUM
eurjchem-1783	327	26	-	-	PUNCT
eurjchem-1783	327	27	chloroalkan-2	chloroalkan-2	NUM
eurjchem-1783	327	28	-	-	PUNCT
eurjchem-1783	327	29	yl	yl	NOUN
eurjchem-1783	327	30	-	-	PUNCT
eurjchem-1783	327	31	chloroformates	chloroformate	NOUN
eurjchem-1783	327	32	.	.	PUNCT
eurjchem-1783	328	1	few	few	ADJ
eurjchem-1783	328	2	of	of	ADP
eurjchem-1783	328	3	the	the	DET
eurjchem-1783	328	4	medicinal	medicinal	ADJ
eurjchem-1783	328	5	industrial	industrial	ADJ
eurjchem-1783	328	6	methods	method	NOUN
eurjchem-1783	328	7	follow	follow	VERB
eurjchem-1783	328	8	the	the	DET
eurjchem-1783	328	9	conversion	conversion	NOUN
eurjchem-1783	328	10	of	of	ADP
eurjchem-1783	328	11	oxazolidinone	oxazolidinone	NOUN
eurjchem-1783	328	12	methyl	methyl	NOUN
eurjchem-1783	328	13	alcohol	alcohol	NOUN
eurjchem-1783	328	14	to	to	ADP
eurjchem-1783	328	15	methyl	methyl	NOUN
eurjchem-1783	328	16	sulphonyl	sulphonyl	NOUN
eurjchem-1783	328	17	group	group	NOUN
eurjchem-1783	328	18	,	,	PUNCT
eurjchem-1783	328	19	azide	azide	NOUN
eurjchem-1783	328	20	,	,	PUNCT
eurjchem-1783	328	21	reduction	reduction	NOUN
eurjchem-1783	328	22	followed	follow	VERB
eurjchem-1783	328	23	by	by	ADP
eurjchem-1783	328	24	acetylation	acetylation	NOUN
eurjchem-1783	328	25	of	of	ADP
eurjchem-1783	328	26	amine	amine	ADJ
eurjchem-1783	328	27	group	group	NOUN
eurjchem-1783	328	28	.	.	PUNCT
eurjchem-1783	329	1	over	over	ADP
eurjchem-1783	329	2	all	all	ADV
eurjchem-1783	329	3	by	by	ADP
eurjchem-1783	329	4	employing	employ	VERB
eurjchem-1783	329	5	our	our	PRON
eurjchem-1783	329	6	new	new	ADJ
eurjchem-1783	329	7	simple	simple	ADJ
eurjchem-1783	329	8	strategies	strategy	NOUN
eurjchem-1783	329	9	,	,	PUNCT
eurjchem-1783	329	10	the	the	DET
eurjchem-1783	329	11	cumbersome	cumbersome	ADJ
eurjchem-1783	329	12	synthesis	synthesis	NOUN
eurjchem-1783	329	13	of	of	ADP
eurjchem-1783	329	14	linezolid	linezolid	NOUN
eurjchem-1783	329	15	and	and	CCONJ
eurjchem-1783	329	16	eperezolid	eperezolid	NOUN
eurjchem-1783	329	17	have	have	AUX
eurjchem-1783	329	18	turned	turn	VERB
eurjchem-1783	329	19	relaxed	relaxed	ADJ
eurjchem-1783	329	20	,	,	PUNCT
eurjchem-1783	329	21	inexpensive	inexpensive	ADJ
eurjchem-1783	329	22	and	and	CCONJ
eurjchem-1783	329	23	crisp	crisp	ADJ
eurjchem-1783	329	24	in	in	ADP
eurjchem-1783	329	25	many	many	ADJ
eurjchem-1783	329	26	aspects	aspect	NOUN
eurjchem-1783	329	27	of	of	ADP
eurjchem-1783	329	28	synthetic	synthetic	ADJ
eurjchem-1783	329	29	chemistry	chemistry	NOUN
eurjchem-1783	329	30	.	.	PUNCT
eurjchem-1783	330	1	in	in	ADP
eurjchem-1783	330	2	summary	summary	NOUN
eurjchem-1783	330	3	,	,	PUNCT
eurjchem-1783	330	4	we	we	PRON
eurjchem-1783	330	5	describe	describe	VERB
eurjchem-1783	330	6	herein	herein	NOUN
eurjchem-1783	330	7	a	a	DET
eurjchem-1783	330	8	simple	simple	ADJ
eurjchem-1783	330	9	,	,	PUNCT
eurjchem-1783	330	10	mild	mild	ADJ
eurjchem-1783	330	11	and	and	CCONJ
eurjchem-1783	330	12	facile	facile	ADJ
eurjchem-1783	330	13	synthesis	synthesis	NOUN
eurjchem-1783	330	14	of	of	ADP
eurjchem-1783	330	15	linezolid	linezolid	NOUN
eurjchem-1783	330	16	and	and	CCONJ
eurjchem-1783	330	17	eperezolid	eperezolid	NOUN
eurjchem-1783	330	18	using	use	VERB
eurjchem-1783	330	19	handy	handy	ADJ
eurjchem-1783	330	20	reaction	reaction	NOUN
eurjchem-1783	330	21	conditions	condition	NOUN
eurjchem-1783	330	22	.	.	PUNCT
eurjchem-1783	331	1	4	4	X
eurjchem-1783	331	2	.	.	X
eurjchem-1783	331	3	conclusions	conclusion	NOUN
eurjchem-1783	331	4	in	in	ADP
eurjchem-1783	331	5	conclusion	conclusion	NOUN
eurjchem-1783	331	6	,	,	PUNCT
eurjchem-1783	331	7	we	we	PRON
eurjchem-1783	331	8	have	have	AUX
eurjchem-1783	331	9	designed	design	VERB
eurjchem-1783	331	10	shortest	short	ADJ
eurjchem-1783	331	11	and	and	CCONJ
eurjchem-1783	331	12	a	a	DET
eurjchem-1783	331	13	simple	simple	ADJ
eurjchem-1783	331	14	synthetic	synthetic	ADJ
eurjchem-1783	331	15	route	route	NOUN
eurjchem-1783	331	16	to	to	PART
eurjchem-1783	331	17	reach	reach	VERB
eurjchem-1783	331	18	oxazolidinone	oxazolidinone	NOUN
eurjchem-1783	331	19	drugs	drug	NOUN
eurjchem-1783	331	20	linezolid	linezolid	NOUN
eurjchem-1783	331	21	and	and	CCONJ
eurjchem-1783	331	22	eperezolid	eperezolid	NOUN
eurjchem-1783	331	23	using	use	VERB
eurjchem-1783	331	24	reagents	reagent	NOUN
eurjchem-1783	331	25	which	which	PRON
eurjchem-1783	331	26	can	can	AUX
eurjchem-1783	331	27	be	be	AUX
eurjchem-1783	331	28	handled	handle	VERB
eurjchem-1783	331	29	easily	easily	ADV
eurjchem-1783	331	30	with	with	ADP
eurjchem-1783	331	31	the	the	DET
eurjchem-1783	331	32	overall	overall	ADJ
eurjchem-1783	331	33	yield	yield	NOUN
eurjchem-1783	331	34	of	of	ADP
eurjchem-1783	331	35	95	95	NUM
eurjchem-1783	331	36	%	%	NOUN
eurjchem-1783	331	37	.	.	PUNCT
eurjchem-1783	332	1	this	this	DET
eurjchem-1783	332	2	method	method	NOUN
eurjchem-1783	332	3	can	can	AUX
eurjchem-1783	332	4	be	be	AUX
eurjchem-1783	332	5	versatile	versatile	ADJ
eurjchem-1783	332	6	in	in	ADP
eurjchem-1783	332	7	the	the	DET
eurjchem-1783	332	8	organic	organic	ADJ
eurjchem-1783	332	9	synthesis	synthesis	NOUN
eurjchem-1783	332	10	of	of	ADP
eurjchem-1783	332	11	linezolid	linezolid	NOUN
eurjchem-1783	332	12	and	and	CCONJ
eurjchem-1783	332	13	eperezolid	eperezolid	NOUN
eurjchem-1783	332	14	derivatives	derivative	NOUN
eurjchem-1783	332	15	and	and	CCONJ
eurjchem-1783	332	16	can	can	AUX
eurjchem-1783	332	17	be	be	AUX
eurjchem-1783	332	18	applied	apply	VERB
eurjchem-1783	332	19	to	to	ADP
eurjchem-1783	332	20	large	large	ADJ
eurjchem-1783	332	21	scale	scale	NOUN
eurjchem-1783	332	22	industrial	industrial	ADJ
eurjchem-1783	332	23	production	production	NOUN
eurjchem-1783	332	24	.	.	PUNCT
eurjchem-1783	333	1	by	by	ADP
eurjchem-1783	333	2	using	use	VERB
eurjchem-1783	333	3	2018	2018	NUM
eurjchem-1783	333	4	–	–	PUNCT
eurjchem-1783	333	5	european	european	ADJ
eurjchem-1783	333	6	journal	journal	NOUN
eurjchem-1783	333	7	of	of	ADP
eurjchem-1783	333	8	chemistry	chemistry	NOUN
eurjchem-1783	333	9	–	–	PUNCT
eurjchem-1783	333	10	cc	cc	NOUN
eurjchem-1783	333	11	by	by	ADP
eurjchem-1783	333	12	nc	nc	PROPN
eurjchem-1783	333	13	–	–	PUNCT
eurjchem-1783	333	14	doi	doi	PROPN
eurjchem-1783	333	15	:	:	PUNCT
eurjchem-1783	333	16	10.5155	10.5155	NUM
eurjchem-1783	333	17	/	/	SYM
eurjchem-1783	333	18	eurjchem.9.4.353	eurjchem.9.4.353	PROPN
eurjchem-1783	333	19	-	-	SYM
eurjchem-1783	333	20	359.1783	359.1783	NUM
eurjchem-1783	333	21	siddaraj	siddaraj	ADJ
eurjchem-1783	333	22	et	et	NOUN
eurjchem-1783	333	23	al	al	PROPN
eurjchem-1783	333	24	.	.	PUNCT
eurjchem-1783	333	25	/	/	SYM
eurjchem-1783	333	26	european	european	PROPN
eurjchem-1783	333	27	journal	journal	PROPN
eurjchem-1783	333	28	of	of	ADP
eurjchem-1783	333	29	chemistry	chemistry	NOUN
eurjchem-1783	333	30	9	9	NUM
eurjchem-1783	333	31	(	(	PUNCT
eurjchem-1783	333	32	4	4	NUM
eurjchem-1783	333	33	)	)	PUNCT
eurjchem-1783	333	34	(	(	PUNCT
eurjchem-1783	333	35	2018	2018	NUM
eurjchem-1783	333	36	)	)	PUNCT
eurjchem-1783	333	37	353	353	NUM
eurjchem-1783	333	38	-	-	SYM
eurjchem-1783	333	39	359	359	NUM
eurjchem-1783	333	40	359	359	NUM
eurjchem-1783	333	41	these	these	DET
eurjchem-1783	333	42	conditions	condition	NOUN
eurjchem-1783	333	43	,	,	PUNCT
eurjchem-1783	333	44	an	an	DET
eurjchem-1783	333	45	efficient	efficient	ADJ
eurjchem-1783	333	46	method	method	NOUN
eurjchem-1783	333	47	had	have	AUX
eurjchem-1783	333	48	been	be	AUX
eurjchem-1783	333	49	demonstrated	demonstrate	VERB
eurjchem-1783	333	50	for	for	ADP
eurjchem-1783	333	51	2	2	NUM
eurjchem-1783	333	52	-	-	PUNCT
eurjchem-1783	333	53	oxazolidinone	oxazolidinone	NOUN
eurjchem-1783	333	54	ring	ring	NOUN
eurjchem-1783	333	55	construction	construction	NOUN
eurjchem-1783	333	56	and	and	CCONJ
eurjchem-1783	333	57	express	express	VERB
eurjchem-1783	333	58	way	way	NOUN
eurjchem-1783	333	59	to	to	PART
eurjchem-1783	333	60	introduce	introduce	VERB
eurjchem-1783	333	61	amide	amide	NOUN
eurjchem-1783	333	62	functionality	functionality	NOUN
eurjchem-1783	333	63	.	.	PUNCT
eurjchem-1783	334	1	the	the	DET
eurjchem-1783	334	2	applicability	applicability	NOUN
eurjchem-1783	334	3	of	of	ADP
eurjchem-1783	334	4	this	this	DET
eurjchem-1783	334	5	approach	approach	NOUN
eurjchem-1783	334	6	was	be	AUX
eurjchem-1783	334	7	shown	show	VERB
eurjchem-1783	334	8	by	by	ADP
eurjchem-1783	334	9	the	the	DET
eurjchem-1783	334	10	synthesis	synthesis	NOUN
eurjchem-1783	334	11	of	of	ADP
eurjchem-1783	334	12	linezolid	linezolid	NOUN
eurjchem-1783	334	13	and	and	CCONJ
eurjchem-1783	334	14	eperazolid	eperazolid	NOUN
eurjchem-1783	334	15	.	.	PUNCT
eurjchem-1783	335	1	we	we	PRON
eurjchem-1783	335	2	hope	hope	VERB
eurjchem-1783	335	3	this	this	DET
eurjchem-1783	335	4	approach	approach	NOUN
eurjchem-1783	335	5	is	be	AUX
eurjchem-1783	335	6	not	not	PART
eurjchem-1783	335	7	only	only	ADV
eurjchem-1783	335	8	restricted	restrict	VERB
eurjchem-1783	335	9	to	to	ADP
eurjchem-1783	335	10	linezolid	linezolid	VERB
eurjchem-1783	335	11	and	and	CCONJ
eurjchem-1783	335	12	eperezolid	eperezolid	NOUN
eurjchem-1783	335	13	,	,	PUNCT
eurjchem-1783	335	14	it	it	PRON
eurjchem-1783	335	15	can	can	AUX
eurjchem-1783	335	16	be	be	AUX
eurjchem-1783	335	17	extended	extend	VERB
eurjchem-1783	335	18	to	to	ADP
eurjchem-1783	335	19	other	other	ADJ
eurjchem-1783	335	20	oxozolidinone	oxozolidinone	NOUN
eurjchem-1783	335	21	drugs	drug	NOUN
eurjchem-1783	335	22	available	available	ADJ
eurjchem-1783	335	23	in	in	ADP
eurjchem-1783	335	24	the	the	DET
eurjchem-1783	335	25	market	market	NOUN
eurjchem-1783	335	26	.	.	PUNCT
eurjchem-1783	336	1	disclosure	disclosure	NOUN
eurjchem-1783	336	2	statement	statement	NOUN
eurjchem-1783	336	3	conflict	conflict	NOUN
eurjchem-1783	336	4	of	of	ADP
eurjchem-1783	336	5	interests	interest	NOUN
eurjchem-1783	336	6	:	:	PUNCT
eurjchem-1783	336	7	the	the	DET
eurjchem-1783	336	8	authors	author	NOUN
eurjchem-1783	336	9	declare	declare	VERB
eurjchem-1783	336	10	that	that	SCONJ
eurjchem-1783	336	11	they	they	PRON
eurjchem-1783	336	12	have	have	VERB
eurjchem-1783	336	13	no	no	DET
eurjchem-1783	336	14	conflict	conflict	NOUN
eurjchem-1783	336	15	of	of	ADP
eurjchem-1783	336	16	interest	interest	NOUN
eurjchem-1783	336	17	.	.	PUNCT
eurjchem-1783	337	1	author	author	NOUN
eurjchem-1783	337	2	contributions	contribution	NOUN
eurjchem-1783	337	3	:	:	PUNCT
eurjchem-1783	337	4	all	all	DET
eurjchem-1783	337	5	authors	author	NOUN
eurjchem-1783	337	6	contributed	contribute	VERB
eurjchem-1783	337	7	equally	equally	ADV
eurjchem-1783	337	8	to	to	ADP
eurjchem-1783	337	9	this	this	DET
eurjchem-1783	337	10	work	work	NOUN
eurjchem-1783	337	11	.	.	PUNCT
eurjchem-1783	338	1	ethical	ethical	ADJ
eurjchem-1783	338	2	approval	approval	NOUN
eurjchem-1783	338	3	:	:	PUNCT
eurjchem-1783	339	1	all	all	DET
eurjchem-1783	339	2	ethical	ethical	ADJ
eurjchem-1783	339	3	guidelines	guideline	NOUN
eurjchem-1783	339	4	have	have	AUX
eurjchem-1783	339	5	been	be	AUX
eurjchem-1783	339	6	adhered	adhere	VERB
eurjchem-1783	339	7	.	.	PUNCT
eurjchem-1783	340	1	sample	sample	NOUN
eurjchem-1783	340	2	availability	availability	NOUN
eurjchem-1783	340	3	:	:	PUNCT
eurjchem-1783	340	4	samples	sample	NOUN
eurjchem-1783	340	5	of	of	ADP
eurjchem-1783	340	6	the	the	DET
eurjchem-1783	340	7	compounds	compound	NOUN
eurjchem-1783	340	8	are	be	AUX
eurjchem-1783	340	9	available	available	ADJ
eurjchem-1783	340	10	from	from	ADP
eurjchem-1783	340	11	the	the	DET
eurjchem-1783	340	12	author	author	NOUN
eurjchem-1783	340	13	.	.	PUNCT
eurjchem-1783	341	1	orcid	orcid	PROPN
eurjchem-1783	341	2	ranjith	ranjith	PROPN
eurjchem-1783	341	3	siddaraj	siddaraj	PROPN
eurjchem-1783	341	4	http://orcid.org/0000-0002-4780-9144	http://orcid.org/0000-0002-4780-9144	PROPN
eurjchem-1783	341	5	shivaraja	shivaraja	NOUN
eurjchem-1783	341	6	govindaiah	govindaiah	PROPN
eurjchem-1783	341	7	http://orcid.org/0000-0001-7545-4611	http://orcid.org/0000-0001-7545-4611	PROPN
eurjchem-1783	341	8	raghu	raghu	PROPN
eurjchem-1783	341	9	ningegowda	ningegowda	PROPN
eurjchem-1783	341	10	http://orcid.org/0000-0003-4817-4061	http://orcid.org/0000-0003-4817-4061	VERB
eurjchem-1783	341	11	nanjunda	nanjunda	PROPN
eurjchem-1783	341	12	swamy	swamy	PROPN
eurjchem-1783	341	13	shivananju	shivananju	NOUN
eurjchem-1783	341	14	http://orcid.org/0000-0002-5494-9428	http://orcid.org/0000-0002-5494-9428	PROPN
eurjchem-1783	341	15	babu	babu	PROPN
eurjchem-1783	341	16	shubha	shubha	PROPN
eurjchem-1783	341	17	priya	priya	PROPN
eurjchem-1783	341	18	http://orcid.org/0000-0003-1110-0771	http://orcid.org/0000-0003-1110-0771	PROPN
eurjchem-1783	341	19	references	reference	NOUN
eurjchem-1783	341	20	[	[	X
eurjchem-1783	341	21	1	1	NUM
eurjchem-1783	341	22	]	]	PUNCT
eurjchem-1783	341	23	.	.	PUNCT
eurjchem-1783	342	1	wallace	wallace	PROPN
eurjchem-1783	342	2	,	,	PUNCT
eurjchem-1783	342	3	r.	r.	PROPN
eurjchem-1783	342	4	j.	j.	PROPN
eurjchem-1783	342	5	j.	j.	PROPN
eurjchem-1783	342	6	;	;	PUNCT
eurjchem-1783	342	7	brown	brown	PROPN
eurjchem-1783	342	8	-	-	PUNCT
eurjchem-1783	342	9	elliott	elliott	PROPN
eurjchem-1783	342	10	,	,	PUNCT
eurjchem-1783	342	11	b.	b.	PROPN
eurjchem-1783	342	12	a.	a.	PROPN
eurjchem-1783	342	13	;	;	PUNCT
eurjchem-1783	342	14	ward	ward	PROPN
eurjchem-1783	342	15	,	,	PUNCT
eurjchem-1783	342	16	s.	s.	PROPN
eurjchem-1783	342	17	c.	c.	PROPN
eurjchem-1783	342	18	;	;	PUNCT
eurjchem-1783	342	19	crist	crist	PROPN
eurjchem-1783	342	20	,	,	PUNCT
eurjchem-1783	342	21	c.	c.	PROPN
eurjchem-1783	342	22	j.	j.	PROPN
eurjchem-1783	342	23	;	;	PUNCT
eurjchem-1783	342	24	mann	mann	PROPN
eurjchem-1783	342	25	,	,	PUNCT
eurjchem-1783	342	26	l.	l.	PROPN
eurjchem-1783	342	27	b.	b.	PROPN
eurjchem-1783	342	28	;	;	PUNCT
eurjchem-1783	342	29	wilson	wilson	PROPN
eurjchem-1783	342	30	,	,	PUNCT
eurjchem-1783	342	31	r.	r.	PROPN
eurjchem-1783	342	32	w.	w.	PROPN
eurjchem-1783	342	33	antimicrob	antimicrob	PROPN
eurjchem-1783	342	34	.	.	PUNCT
eurjchem-1783	343	1	agents	agents	PROPN
eurjchem-1783	343	2	chemother	chemother	PROPN
eurjchem-1783	343	3	.	.	PUNCT
eurjchem-1783	344	1	2001	2001	NUM
eurjchem-1783	344	2	,	,	PUNCT
eurjchem-1783	344	3	45	45	NUM
eurjchem-1783	344	4	,	,	PUNCT
eurjchem-1783	344	5	764	764	NUM
eurjchem-1783	344	6	-	-	SYM
eurjchem-1783	344	7	767	767	NUM
eurjchem-1783	344	8	.	.	PUNCT
eurjchem-1783	345	1	[	[	X
eurjchem-1783	345	2	2	2	NUM
eurjchem-1783	345	3	]	]	PUNCT
eurjchem-1783	345	4	.	.	PUNCT
eurjchem-1783	346	1	peters	peters	PROPN
eurjchem-1783	346	2	,	,	PUNCT
eurjchem-1783	346	3	j.	j.	PROPN
eurjchem-1783	346	4	;	;	PUNCT
eurjchem-1783	346	5	kondo	kondo	PROPN
eurjchem-1783	346	6	,	,	PUNCT
eurjchem-1783	346	7	k.	k.	PROPN
eurjchem-1783	346	8	;	;	PUNCT
eurjchem-1783	346	9	lee	lee	PROPN
eurjchem-1783	346	10	,	,	PUNCT
eurjchem-1783	346	11	r.	r.	PROPN
eurjchem-1783	346	12	;	;	PUNCT
eurjchem-1783	346	13	lin	lin	PROPN
eurjchem-1783	346	14	,	,	PUNCT
eurjchem-1783	346	15	c.	c.	PROPN
eurjchem-1783	346	16	;	;	PUNCT
eurjchem-1783	346	17	inderlied	inderlie	VERB
eurjchem-1783	346	18	,	,	PUNCT
eurjchem-1783	346	19	c.	c.	PROPN
eurjchem-1783	346	20	j.	j.	PROPN
eurjchem-1783	346	21	antimicrob	antimicrob	PROPN
eurjchem-1783	346	22	.	.	PUNCT
eurjchem-1783	347	1	chemother	chemother	PROPN
eurjchem-1783	347	2	.	.	PUNCT
eurjchem-1783	348	1	1995	1995	NUM
eurjchem-1783	348	2	,	,	PUNCT
eurjchem-1783	348	3	35	35	NUM
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eurjchem-1783	351	2	,	,	PUNCT
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eurjchem-1783	351	4	,	,	PUNCT
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eurjchem-1783	351	6	-	-	SYM
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eurjchem-1783	351	8	.	.	PUNCT
eurjchem-1783	352	1	[	[	X
eurjchem-1783	352	2	4	4	NUM
eurjchem-1783	352	3	]	]	PUNCT
eurjchem-1783	352	4	.	.	PUNCT
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eurjchem-1783	354	28	.	.	PUNCT
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eurjchem-1783	355	2	.	.	PUNCT
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eurjchem-1783	356	2	.	.	PUNCT
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eurjchem-1783	357	2	,	,	PUNCT
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eurjchem-1783	357	4	,	,	PUNCT
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eurjchem-1783	357	6	-	-	SYM
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eurjchem-1783	357	8	.	.	PUNCT
eurjchem-1783	358	1	[	[	X
eurjchem-1783	358	2	5	5	NUM
eurjchem-1783	358	3	]	]	PUNCT
eurjchem-1783	358	4	.	.	PUNCT
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eurjchem-1783	359	2	,	,	PUNCT
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eurjchem-1783	359	5	;	;	PUNCT
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eurjchem-1783	359	7	,	,	PUNCT
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eurjchem-1783	359	19	;	;	PUNCT
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eurjchem-1783	359	21	,	,	PUNCT
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eurjchem-1783	359	25	,	,	PUNCT
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eurjchem-1783	359	27	;	;	PUNCT
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eurjchem-1783	359	30	a.	a.	PROPN
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eurjchem-1783	359	35	.	.	PUNCT
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eurjchem-1783	360	2	,	,	PUNCT
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eurjchem-1783	360	4	,	,	PUNCT
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eurjchem-1783	360	6	-	-	SYM
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eurjchem-1783	360	8	.	.	PUNCT
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eurjchem-1783	361	2	6	6	NUM
eurjchem-1783	361	3	]	]	PUNCT
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eurjchem-1783	361	8	;	;	PUNCT
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eurjchem-1783	362	2	,	,	PUNCT
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eurjchem-1783	362	4	,	,	PUNCT
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eurjchem-1783	362	6	-	-	SYM
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eurjchem-1783	363	1	[	[	X
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eurjchem-1783	363	4	.	.	PUNCT
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eurjchem-1783	363	15	k.	k.	PROPN
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eurjchem-1783	365	6	-	-	SYM
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eurjchem-1783	365	8	.	.	PUNCT
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eurjchem-1783	416	3	rao	rao	PROPN
eurjchem-1783	416	4	,	,	PUNCT
eurjchem-1783	416	5	d.	d.	PROPN
eurjchem-1783	416	6	;	;	PUNCT
eurjchem-1783	416	7	krishna	krishna	PROPN
eurjchem-1783	416	8	,	,	PUNCT
eurjchem-1783	416	9	r.	r.	PROPN
eurjchem-1783	416	10	p.	p.	PROPN
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eurjchem-1783	416	12	int	int	PROPN
eurjchem-1783	416	13	.	.	PUNCT
eurjchem-1783	417	1	appl	appl	PROPN
eurjchem-1783	417	2	.	.	PROPN
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eurjchem-1783	417	4	,	,	PUNCT
eurjchem-1783	417	5	2005	2005	NUM
eurjchem-1783	417	6	;	;	PUNCT
eurjchem-1783	418	1	chem	chem	NOUN
eurjchem-1783	418	2	.	.	PUNCT
eurjchem-1783	419	1	abstr	abstr	PROPN
eurjchem-1783	419	2	.	.	PUNCT
eurjchem-1783	420	1	2005	2005	NUM
eurjchem-1783	420	2	,	,	PUNCT
eurjchem-1783	420	3	143	143	NUM
eurjchem-1783	420	4	,	,	PUNCT
eurjchem-1783	420	5	440395	440395	NUM
eurjchem-1783	420	6	.	.	PUNCT
eurjchem-1783	421	1	[	[	X
eurjchem-1783	421	2	21	21	NUM
eurjchem-1783	421	3	]	]	PUNCT
eurjchem-1783	421	4	.	.	PUNCT
eurjchem-1783	422	1	mohan	mohan	PROPN
eurjchem-1783	422	2	-	-	PUNCT
eurjchem-1783	422	3	rao	rao	PROPN
eurjchem-1783	422	4	,	,	PUNCT
eurjchem-1783	422	5	d.	d.	PROPN
eurjchem-1783	422	6	;	;	PUNCT
eurjchem-1783	422	7	krishna	krishna	PROPN
eurjchem-1783	422	8	,	,	PUNCT
eurjchem-1783	422	9	r.	r.	PROPN
eurjchem-1783	422	10	p.	p.	PROPN
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eurjchem-1783	422	12	int	int	PROPN
eurjchem-1783	422	13	.	.	PUNCT
eurjchem-1783	423	1	appl	appl	PROPN
eurjchem-1783	423	2	.	.	PROPN
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eurjchem-1783	423	4	,	,	PUNCT
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eurjchem-1783	423	6	;	;	PUNCT
eurjchem-1783	424	1	chem	chem	NOUN
eurjchem-1783	424	2	.	.	PUNCT
eurjchem-1783	425	1	abstr	abstr	PROPN
eurjchem-1783	425	2	.	.	PUNCT
eurjchem-1783	426	1	2006	2006	NUM
eurjchem-1783	426	2	,	,	PUNCT
eurjchem-1783	426	3	144	144	NUM
eurjchem-1783	426	4	,	,	PUNCT
eurjchem-1783	426	5	170978	170978	NUM
eurjchem-1783	426	6	.	.	PUNCT
eurjchem-1783	427	1	[	[	X
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eurjchem-1783	427	3	]	]	SYM
eurjchem-1783	427	4	.	.	PUNCT
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eurjchem-1783	427	6	,	,	PUNCT
eurjchem-1783	427	7	g.	g.	PROPN
eurjchem-1783	427	8	;	;	PUNCT
eurjchem-1783	427	9	om	om	PROPN
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eurjchem-1783	427	11	,	,	PUNCT
eurjchem-1783	427	12	g.	g.	PROPN
eurjchem-1783	427	13	;	;	PUNCT
eurjchem-1783	427	14	ramanatham	ramanatham	PROPN
eurjchem-1783	427	15	,	,	PUNCT
eurjchem-1783	427	16	j.	j.	PROPN
eurjchem-1783	427	17	;	;	PUNCT
eurjchem-1783	427	18	dubey	dubey	PROPN
eurjchem-1783	427	19	,	,	PUNCT
eurjchem-1783	427	20	p.	p.	PROPN
eurjchem-1783	427	21	k.	k.	PROPN
eurjchem-1783	428	1	indian	indian	PROPN
eurjchem-1783	428	2	j.	j.	PROPN
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eurjchem-1783	428	4	.	.	PUNCT
eurjchem-1783	429	1	2005	2005	NUM
eurjchem-1783	429	2	,	,	PUNCT
eurjchem-1783	429	3	44b	44b	NUM
eurjchem-1783	429	4	,	,	PUNCT
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eurjchem-1783	429	6	-	-	SYM
eurjchem-1783	429	7	1238	1238	NUM
eurjchem-1783	429	8	.	.	PUNCT
eurjchem-1783	430	1	[	[	X
eurjchem-1783	430	2	23	23	NUM
eurjchem-1783	430	3	]	]	SYM
eurjchem-1783	430	4	.	.	PUNCT
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eurjchem-1783	430	6	,	,	PUNCT
eurjchem-1783	430	7	g.	g.	PROPN
eurjchem-1783	430	8	;	;	PUNCT
eurjchem-1783	430	9	om	om	PROPN
eurjchem-1783	430	10	reddy	reddy	PROPN
eurjchem-1783	430	11	,	,	PUNCT
eurjchem-1783	430	12	g.	g.	PROPN
eurjchem-1783	430	13	;	;	PUNCT
eurjchem-1783	430	14	rajesh	rajesh	PROPN
eurjchem-1783	430	15	,	,	PUNCT
eurjchem-1783	430	16	t.	t.	PROPN
eurjchem-1783	430	17	;	;	PUNCT
eurjchem-1783	430	18	ramanatham	ramanatham	PROPN
eurjchem-1783	430	19	,	,	PUNCT
eurjchem-1783	430	20	j.	j.	PROPN
eurjchem-1783	430	21	;	;	PUNCT
eurjchem-1783	430	22	dubey	dubey	PROPN
eurjchem-1783	430	23	,	,	PUNCT
eurjchem-1783	430	24	p.	p.	PROPN
eurjchem-1783	430	25	k.	k.	PROPN
eurjchem-1783	431	1	tetrahedron	tetrahedron	PROPN
eurjchem-1783	431	2	lett	lett	PROPN
eurjchem-1783	431	3	.	.	PUNCT
eurjchem-1783	431	4	2008	2008	NUM
eurjchem-1783	431	5	,	,	PUNCT
eurjchem-1783	431	6	49	49	NUM
eurjchem-1783	431	7	,	,	PUNCT
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eurjchem-1783	431	9	-	-	SYM
eurjchem-1783	431	10	3062	3062	NUM
eurjchem-1783	431	11	.	.	PUNCT
eurjchem-1783	432	1	[	[	X
eurjchem-1783	432	2	24	24	NUM
eurjchem-1783	432	3	]	]	PUNCT
eurjchem-1783	432	4	.	.	PUNCT
eurjchem-1783	433	1	rajesh	rajesh	PROPN
eurjchem-1783	433	2	,	,	PUNCT
eurjchem-1783	433	3	t.	t.	PROPN
eurjchem-1783	433	4	;	;	PUNCT
eurjchem-1783	433	5	narayana	narayana	PROPN
eurjchem-1783	433	6	rao	rao	PROPN
eurjchem-1783	433	7	,	,	PUNCT
eurjchem-1783	433	8	s.	s.	PROPN
eurjchem-1783	433	9	p.	p.	PROPN
eurjchem-1783	433	10	;	;	PUNCT
eurjchem-1783	433	11	suresh	suresh	PROPN
eurjchem-1783	433	12	,	,	PUNCT
eurjchem-1783	433	13	k.	k.	PROPN
eurjchem-1783	433	14	madhusudhan	madhusudhan	PROPN
eurjchem-1783	433	15	,	,	PUNCT
eurjchem-1783	433	16	g.	g.	PROPN
eurjchem-1783	433	17	;	;	PUNCT
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eurjchem-1783	433	21	j.	j.	PROPN
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eurjchem-1783	433	24	.	.	PUNCT
eurjchem-1783	434	1	2010	2010	NUM
eurjchem-1783	434	2	,	,	PUNCT
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eurjchem-1783	434	4	,	,	PUNCT
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eurjchem-1783	434	6	-	-	SYM
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eurjchem-1783	434	8	.	.	PUNCT
eurjchem-1783	435	1	[	[	X
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eurjchem-1783	435	3	]	]	PUNCT
eurjchem-1783	435	4	.	.	PUNCT
eurjchem-1783	436	1	moran	moran	PROPN
eurjchem-1783	436	2	-	-	PUNCT
eurjchem-1783	436	3	ramallal	ramallal	PROPN
eurjchem-1783	436	4	,	,	PUNCT
eurjchem-1783	436	5	r.	r.	PROPN
eurjchem-1783	436	6	;	;	PUNCT
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eurjchem-1783	436	10	;	;	PUNCT
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eurjchem-1783	436	12	,	,	PUNCT
eurjchem-1783	436	13	v.	v.	X
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eurjchem-1783	436	15	.	.	PUNCT
eurjchem-1783	437	1	lett	lett	PROPN
eurjchem-1783	437	2	.	.	PROPN
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eurjchem-1783	437	4	,	,	PUNCT
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eurjchem-1783	437	6	,	,	PUNCT
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eurjchem-1783	437	8	-	-	SYM
eurjchem-1783	437	9	1938	1938	NUM
eurjchem-1783	437	10	.	.	PUNCT
eurjchem-1783	438	1	[	[	X
eurjchem-1783	438	2	26	26	NUM
eurjchem-1783	438	3	]	]	PUNCT
eurjchem-1783	438	4	.	.	PUNCT
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eurjchem-1783	439	2	,	,	PUNCT
eurjchem-1783	439	3	b.	b.	PROPN
eurjchem-1783	439	4	;	;	PUNCT
eurjchem-1783	439	5	rajesh	rajesh	PROPN
eurjchem-1783	439	6	,	,	PUNCT
eurjchem-1783	439	7	b.	b.	PROPN
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eurjchem-1783	439	9	;	;	PUNCT
eurjchem-1783	439	10	rajamohan	rajamohan	ADV
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eurjchem-1783	439	12	r.	r.	PROPN
eurjchem-1783	439	13	p.	p.	PROPN
eurjchem-1783	439	14	;	;	PUNCT
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eurjchem-1783	439	16	,	,	PUNCT
eurjchem-1783	439	17	d.	d.	PROPN
eurjchem-1783	439	18	;	;	PUNCT
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eurjchem-1783	439	21	t.	t.	PROPN
eurjchem-1783	439	22	org	org	PROPN
eurjchem-1783	439	23	.	.	PUNCT
eurjchem-1783	440	1	lett	lett	PROPN
eurjchem-1783	440	2	.	.	PROPN
eurjchem-1783	441	1	2003	2003	NUM
eurjchem-1783	441	2	,	,	PUNCT
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eurjchem-1783	441	4	,	,	PUNCT
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eurjchem-1783	441	6	-	-	SYM
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eurjchem-1783	441	8	.	.	PUNCT
eurjchem-1783	442	1	[	[	X
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eurjchem-1783	442	3	]	]	PUNCT
eurjchem-1783	442	4	.	.	PUNCT
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eurjchem-1783	443	2	,	,	PUNCT
eurjchem-1783	443	3	n.	n.	PROPN
eurjchem-1783	443	4	;	;	PUNCT
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eurjchem-1783	443	7	d.	d.	PROPN
eurjchem-1783	443	8	;	;	PUNCT
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eurjchem-1783	443	11	k.	k.	PROPN
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eurjchem-1783	443	13	;	;	PUNCT
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eurjchem-1783	443	16	k.	k.	PROPN
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eurjchem-1783	443	18	;	;	PUNCT
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eurjchem-1783	443	25	;	;	PUNCT
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eurjchem-1783	443	29	;	;	PUNCT
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eurjchem-1783	443	43	;	;	PUNCT
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eurjchem-1783	443	51	;	;	PUNCT
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eurjchem-1783	444	2	,	,	PUNCT
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eurjchem-1783	444	4	,	,	PUNCT
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eurjchem-1783	444	6	-	-	SYM
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eurjchem-1783	444	8	.	.	PUNCT
eurjchem-1783	445	1	[	[	X
eurjchem-1783	445	2	28	28	NUM
eurjchem-1783	445	3	]	]	PUNCT
eurjchem-1783	445	4	.	.	PUNCT
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eurjchem-1783	446	2	,	,	PUNCT
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eurjchem-1783	446	4	;	;	PUNCT
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eurjchem-1783	446	6	,	,	PUNCT
eurjchem-1783	446	7	y.	y.	PROPN
eurjchem-1783	446	8	;	;	PUNCT
eurjchem-1783	446	9	tomita	tomita	PROPN
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eurjchem-1783	446	12	;	;	PUNCT
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eurjchem-1783	446	20	;	;	PUNCT
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eurjchem-1783	446	24	;	;	PUNCT
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eurjchem-1783	446	28	;	;	PUNCT
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eurjchem-1783	446	32	;	;	PUNCT
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eurjchem-1783	446	35	o.	o.	PROPN
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eurjchem-1783	448	2	.	.	PUNCT
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eurjchem-1783	449	2	,	,	PUNCT
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eurjchem-1783	449	6	-	-	SYM
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eurjchem-1783	449	8	.	.	PUNCT
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eurjchem-1783	451	5	and	and	CCONJ
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eurjchem-1783	451	18	.	.	PUNCT
eurjchem-1783	452	1	the	the	DET
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eurjchem-1783	452	4	of	of	ADP
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eurjchem-1783	452	17	-	-	PUNCT
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eurjchem-1783	452	20	(	(	PUNCT
eurjchem-1783	452	21	cc	cc	NOUN
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eurjchem-1783	452	23	nc	nc	PROPN
eurjchem-1783	452	24	)	)	PUNCT
eurjchem-1783	452	25	(	(	PUNCT
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eurjchem-1783	452	31	(	(	PUNCT
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eurjchem-1783	452	33	)	)	PUNCT
eurjchem-1783	452	34	.	.	PUNCT
eurjchem-1783	453	1	by	by	ADP
eurjchem-1783	453	2	accessing	access	VERB
eurjchem-1783	453	3	the	the	DET
eurjchem-1783	453	4	work	work	NOUN
eurjchem-1783	453	5	,	,	PUNCT
eurjchem-1783	453	6	you	you	PRON
eurjchem-1783	453	7	hereby	hereby	ADV
eurjchem-1783	453	8	accept	accept	VERB
eurjchem-1783	453	9	the	the	DET
eurjchem-1783	453	10	terms	term	NOUN
eurjchem-1783	453	11	.	.	PUNCT
eurjchem-1783	454	1	this	this	PRON
eurjchem-1783	454	2	is	be	AUX
eurjchem-1783	454	3	an	an	DET
eurjchem-1783	454	4	open	open	ADJ
eurjchem-1783	454	5	access	access	NOUN
eurjchem-1783	454	6	article	article	NOUN
eurjchem-1783	454	7	distributed	distribute	VERB
eurjchem-1783	454	8	under	under	ADP
eurjchem-1783	454	9	the	the	DET
eurjchem-1783	454	10	terms	term	NOUN
eurjchem-1783	454	11	and	and	CCONJ
eurjchem-1783	454	12	conditions	condition	NOUN
eurjchem-1783	454	13	of	of	ADP
eurjchem-1783	454	14	the	the	DET
eurjchem-1783	454	15	cc	cc	PROPN
eurjchem-1783	454	16	by	by	ADP
eurjchem-1783	454	17	nc	nc	PROPN
eurjchem-1783	454	18	license	license	PROPN
eurjchem-1783	454	19	,	,	PUNCT
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eurjchem-1783	454	21	permits	permit	VERB
eurjchem-1783	454	22	unrestricted	unrestricted	ADJ
eurjchem-1783	454	23	non	non	ADJ
eurjchem-1783	454	24	-	-	ADJ
eurjchem-1783	454	25	commercial	commercial	ADJ
eurjchem-1783	454	26	use	use	NOUN
eurjchem-1783	454	27	,	,	PUNCT
eurjchem-1783	454	28	distribution	distribution	NOUN
eurjchem-1783	454	29	,	,	PUNCT
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eurjchem-1783	454	31	reproduction	reproduction	NOUN
eurjchem-1783	454	32	in	in	ADP
eurjchem-1783	454	33	any	any	DET
eurjchem-1783	454	34	medium	medium	NOUN
eurjchem-1783	454	35	,	,	PUNCT
eurjchem-1783	454	36	provided	provide	VERB
eurjchem-1783	454	37	the	the	DET
eurjchem-1783	454	38	original	original	ADJ
eurjchem-1783	454	39	work	work	NOUN
eurjchem-1783	454	40	is	be	AUX
eurjchem-1783	454	41	properly	properly	ADV
eurjchem-1783	454	42	cited	cite	VERB
eurjchem-1783	454	43	without	without	ADP
eurjchem-1783	454	44	any	any	DET
eurjchem-1783	454	45	further	further	ADJ
eurjchem-1783	454	46	permission	permission	NOUN
eurjchem-1783	454	47	from	from	ADP
eurjchem-1783	454	48	atlanta	atlanta	PROPN
eurjchem-1783	454	49	publishing	publishing	PROPN
eurjchem-1783	454	50	house	house	PROPN
eurjchem-1783	454	51	llc	llc	PROPN
eurjchem-1783	454	52	(	(	PUNCT
eurjchem-1783	454	53	european	european	PROPN
eurjchem-1783	454	54	journal	journal	PROPN
eurjchem-1783	454	55	of	of	ADP
eurjchem-1783	454	56	chemistry	chemistry	NOUN
eurjchem-1783	454	57	)	)	PUNCT
eurjchem-1783	454	58	.	.	PUNCT
eurjchem-1783	455	1	no	no	DET
eurjchem-1783	455	2	use	use	NOUN
eurjchem-1783	455	3	,	,	PUNCT
eurjchem-1783	455	4	distribution	distribution	NOUN
eurjchem-1783	455	5	or	or	CCONJ
eurjchem-1783	455	6	reproduction	reproduction	NOUN
eurjchem-1783	455	7	is	be	AUX
eurjchem-1783	455	8	permitted	permit	VERB
eurjchem-1783	455	9	which	which	PRON
eurjchem-1783	455	10	does	do	AUX
eurjchem-1783	455	11	not	not	PART
eurjchem-1783	455	12	comply	comply	VERB
eurjchem-1783	455	13	with	with	ADP
eurjchem-1783	455	14	these	these	DET
eurjchem-1783	455	15	terms	term	NOUN
eurjchem-1783	455	16	.	.	PUNCT
eurjchem-1783	456	1	permissions	permission	NOUN
eurjchem-1783	456	2	for	for	ADP
eurjchem-1783	456	3	commercial	commercial	ADJ
eurjchem-1783	456	4	use	use	NOUN
eurjchem-1783	456	5	of	of	ADP
eurjchem-1783	456	6	this	this	DET
eurjchem-1783	456	7	work	work	NOUN
eurjchem-1783	456	8	beyond	beyond	ADP
eurjchem-1783	456	9	the	the	DET
eurjchem-1783	456	10	scope	scope	NOUN
eurjchem-1783	456	11	of	of	ADP
eurjchem-1783	456	12	the	the	DET
eurjchem-1783	456	13	license	license	NOUN
eurjchem-1783	456	14	(	(	PUNCT
eurjchem-1783	456	15	http://www.eurjchem.com/index.php/eurjchem/pages/view/terms	http://www.eurjchem.com/index.php/eurjchem/pages/view/term	NOUN
eurjchem-1783	456	16	)	)	PUNCT
eurjchem-1783	456	17	are	be	AUX
eurjchem-1783	456	18	administered	administer	VERB
eurjchem-1783	456	19	by	by	ADP
eurjchem-1783	456	20	atlanta	atlanta	PROPN
eurjchem-1783	456	21	publishing	publishing	PROPN
eurjchem-1783	456	22	house	house	PROPN
eurjchem-1783	456	23	llc	llc	PROPN
eurjchem-1783	456	24	(	(	PUNCT
eurjchem-1783	456	25	european	european	PROPN
eurjchem-1783	456	26	journal	journal	PROPN
eurjchem-1783	456	27	of	of	ADP
eurjchem-1783	456	28	chemistry	chemistry	NOUN
eurjchem-1783	456	29	)	)	PUNCT
eurjchem-1783	456	30	.	.	PUNCT
eurjchem-1783	457	1	2018	2018	NUM
eurjchem-1783	457	2	–	–	PUNCT
eurjchem-1783	457	3	european	european	ADJ
eurjchem-1783	457	4	journal	journal	NOUN
eurjchem-1783	457	5	of	of	ADP
eurjchem-1783	457	6	chemistry	chemistry	NOUN
eurjchem-1783	457	7	–	–	PUNCT
eurjchem-1783	457	8	cc	cc	NOUN
eurjchem-1783	457	9	by	by	ADP
eurjchem-1783	457	10	nc	nc	PROPN
eurjchem-1783	457	11	–	–	PUNCT
eurjchem-1783	457	12	doi	doi	PROPN
eurjchem-1783	457	13	:	:	PUNCT
eurjchem-1783	457	14	10.5155	10.5155	NUM
eurjchem-1783	457	15	/	/	SYM
eurjchem-1783	457	16	eurjchem.9.4.353	eurjchem.9.4.353	PROPN
eurjchem-1783	457	17	-	-	PUNCT
eurjchem-1783	457	18	359.1783	359.1783	NUM
eurjchem-1783	457	19	http://orcid.org/0000-0002-4780-9144	http://orcid.org/0000-0002-4780-9144	ADJ
eurjchem-1783	457	20	http://orcid.org/0000-0001-7545-4611	http://orcid.org/0000-0001-7545-4611	NOUN
eurjchem-1783	457	21	http://orcid.org/0000-0003-4817-4061	http://orcid.org/0000-0003-4817-4061	NOUN
eurjchem-1783	457	22	http://orcid.org/0000-0002-5494-9428	http://orcid.org/0000-0002-5494-9428	VERB
eurjchem-1783	457	23	http://orcid.org/0000-0003-1110-0771	http://orcid.org/0000-0003-1110-0771	NOUN
eurjchem-1783	457	24	http://www.eurjchem.com/index.php/eurjchem/pages/view/terms	http://www.eurjchem.com/index.php/eurjchem/pages/view/term	NOUN
eurjchem-1783	457	25	http://creativecommons.org/licenses/by-nc/4.0	http://creativecommons.org/licenses/by-nc/4.0	PROPN
eurjchem-1783	457	26	http://www.eurjchem.com/index.php/eurjchem/pages/view/terms	http://www.eurjchem.com/index.php/eurjchem/pages/view/term	NOUN
eurjchem-1783	457	27	1	1	NUM
eurjchem-1783	457	28	.	.	PUNCT
eurjchem-1783	457	29	introduction	introduction	NOUN
eurjchem-1783	457	30	2	2	NUM
eurjchem-1783	457	31	.	.	PUNCT
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eurjchem-1783	457	33	2.1	2.1	NUM
eurjchem-1783	457	34	.	.	PUNCT
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eurjchem-1783	457	36	2.2	2.2	NUM
eurjchem-1783	457	37	.	.	PUNCT
eurjchem-1783	458	1	synthesis	synthesis	NOUN
eurjchem-1783	458	2	2.2.1	2.2.1	NUM
eurjchem-1783	458	3	.	.	PUNCT
eurjchem-1783	458	4	synthesis	synthesis	NOUN
eurjchem-1783	458	5	of	of	ADP
eurjchem-1783	458	6	4-(2	4-(2	PROPN
eurjchem-1783	458	7	-	-	PUNCT
eurjchem-1783	458	8	fluoro-4	fluoro-4	NOUN
eurjchem-1783	458	9	-	-	PUNCT
eurjchem-1783	458	10	nitrophenyl	nitrophenyl	NOUN
eurjchem-1783	458	11	)	)	PUNCT
eurjchem-1783	458	12	morpholine	morpholine	NOUN
eurjchem-1783	458	13	(	(	PUNCT
eurjchem-1783	458	14	1	1	NUM
eurjchem-1783	458	15	)	)	PUNCT
eurjchem-1783	458	16	2.2.2	2.2.2	NUM
eurjchem-1783	458	17	.	.	PUNCT
eurjchem-1783	459	1	synthesis	synthesis	NOUN
eurjchem-1783	459	2	3	3	NUM
eurjchem-1783	459	3	-	-	PUNCT
eurjchem-1783	459	4	fluoro-4	fluoro-4	NOUN
eurjchem-1783	459	5	-	-	PUNCT
eurjchem-1783	459	6	morpholinoaniline	morpholinoaniline	NOUN
eurjchem-1783	459	7	(	(	PUNCT
eurjchem-1783	459	8	2	2	NUM
eurjchem-1783	459	9	)	)	PUNCT
eurjchem-1783	459	10	2.2.3	2.2.3	NUM
eurjchem-1783	459	11	.	.	PUNCT
eurjchem-1783	459	12	synthesis	synthesis	NOUN
eurjchem-1783	459	13	of	of	ADP
eurjchem-1783	459	14	benzyl	benzyl	NOUN
eurjchem-1783	459	15	(	(	PUNCT
eurjchem-1783	459	16	3	3	NUM
eurjchem-1783	459	17	-	-	PUNCT
eurjchem-1783	459	18	fluoro-4	fluoro-4	NOUN
eurjchem-1783	459	19	-	-	PUNCT
eurjchem-1783	459	20	morpholinophenyl	morpholinophenyl	NOUN
eurjchem-1783	459	21	)	)	PUNCT
eurjchem-1783	459	22	carbamate	carbamate	NOUN
eurjchem-1783	459	23	(	(	PUNCT
eurjchem-1783	459	24	3	3	NUM
eurjchem-1783	459	25	)	)	PUNCT
eurjchem-1783	459	26	2.2.4	2.2.4	NUM
eurjchem-1783	459	27	.	.	PUNCT
eurjchem-1783	460	1	synthesis	synthesis	NOUN
eurjchem-1783	460	2	of	of	ADP
eurjchem-1783	460	3	(	(	PUNCT
eurjchem-1783	460	4	r)-5-(bromomethyl)-3-(3	r)-5-(bromomethyl)-3-(3	NOUN
eurjchem-1783	460	5	-	-	PUNCT
eurjchem-1783	460	6	fluoro-4	fluoro-4	NOUN
eurjchem-1783	460	7	-	-	PUNCT
eurjchem-1783	460	8	morpholinophenyl	morpholinophenyl	NOUN
eurjchem-1783	460	9	)	)	PUNCT
eurjchem-1783	460	10	oxazolidin-2	oxazolidin-2	NUM
eurjchem-1783	460	11	-	-	SYM
eurjchem-1783	460	12	one	one	NUM
eurjchem-1783	460	13	(	(	PUNCT
eurjchem-1783	460	14	4	4	NUM
eurjchem-1783	460	15	)	)	PUNCT
eurjchem-1783	460	16	2.2.5	2.2.5	NUM
eurjchem-1783	460	17	.	.	PUNCT
eurjchem-1783	461	1	synthesis	synthesis	NOUN
eurjchem-1783	461	2	of	of	ADP
eurjchem-1783	461	3	(	(	PUNCT
eurjchem-1783	461	4	s)-n-((3-(3	s)-n-((3-(3	PROPN
eurjchem-1783	461	5	-	-	PUNCT
eurjchem-1783	461	6	fluoro-4	fluoro-4	NOUN
eurjchem-1783	461	7	-	-	PUNCT
eurjchem-1783	461	8	morpholinophenyl)-2	morpholinophenyl)-2	NOUN
eurjchem-1783	461	9	-	-	PUNCT
eurjchem-1783	461	10	oxooxazolidin-5	oxooxazolidin-5	NUM
eurjchem-1783	461	11	-	-	PUNCT
eurjchem-1783	461	12	yl	yl	NOUN
eurjchem-1783	461	13	)	)	PUNCT
eurjchem-1783	461	14	methyl	methyl	NOUN
eurjchem-1783	461	15	)	)	PUNCT
eurjchem-1783	461	16	acetamide	acetamide	NOUN
eurjchem-1783	461	17	(	(	PUNCT
eurjchem-1783	461	18	5	5	NUM
eurjchem-1783	461	19	)	)	PUNCT
eurjchem-1783	461	20	2.2.6	2.2.6	NUM
eurjchem-1783	461	21	.	.	PUNCT
eurjchem-1783	461	22	synthesis	synthesis	NOUN
eurjchem-1783	461	23	of	of	ADP
eurjchem-1783	461	24	1-(2	1-(2	PROPN
eurjchem-1783	461	25	-	-	PUNCT
eurjchem-1783	461	26	fluoro-4	fluoro-4	NOUN
eurjchem-1783	461	27	-	-	PUNCT
eurjchem-1783	461	28	nitrophenyl	nitrophenyl	NOUN
eurjchem-1783	461	29	)	)	PUNCT
eurjchem-1783	461	30	piperazine	piperazine	NOUN
eurjchem-1783	461	31	(	(	PUNCT
eurjchem-1783	461	32	6	6	NUM
eurjchem-1783	461	33	)	)	PUNCT
eurjchem-1783	461	34	2.2.7	2.2.7	NUM
eurjchem-1783	461	35	.	.	PUNCT
eurjchem-1783	462	1	synthesis	synthesis	NOUN
eurjchem-1783	462	2	of	of	ADP
eurjchem-1783	462	3	tert	tert	NOUN
eurjchem-1783	462	4	-	-	PUNCT
eurjchem-1783	462	5	butyl	butyl	NOUN
eurjchem-1783	462	6	4-(2	4-(2	PROPN
eurjchem-1783	462	7	-	-	PUNCT
eurjchem-1783	462	8	fluoro-4	fluoro-4	NOUN
eurjchem-1783	462	9	-	-	PUNCT
eurjchem-1783	462	10	nitrophenyl	nitrophenyl	NOUN
eurjchem-1783	462	11	)	)	PUNCT
eurjchem-1783	462	12	piperazine-1	piperazine-1	NOUN
eurjchem-1783	462	13	-	-	NOUN
eurjchem-1783	462	14	carboxylate	carboxylate	NOUN
eurjchem-1783	462	15	(	(	PUNCT
eurjchem-1783	462	16	7	7	NUM
eurjchem-1783	462	17	)	)	PUNCT
eurjchem-1783	462	18	2.2.8	2.2.8	NUM
eurjchem-1783	462	19	.	.	PUNCT
eurjchem-1783	463	1	synthesis	synthesis	NOUN
eurjchem-1783	463	2	of	of	ADP
eurjchem-1783	463	3	tert	tert	NOUN
eurjchem-1783	463	4	-	-	PUNCT
eurjchem-1783	463	5	butyl	butyl	NOUN
eurjchem-1783	463	6	4-(4	4-(4	PROPN
eurjchem-1783	463	7	-	-	PUNCT
eurjchem-1783	463	8	amino-2	amino-2	VERB
eurjchem-1783	463	9	-	-	PUNCT
eurjchem-1783	463	10	fluorophenyl	fluorophenyl	NOUN
eurjchem-1783	463	11	)	)	PUNCT
eurjchem-1783	463	12	piperazine-1	piperazine-1	NOUN
eurjchem-1783	463	13	-	-	NOUN
eurjchem-1783	463	14	carboxylate	carboxylate	NOUN
eurjchem-1783	463	15	(	(	PUNCT
eurjchem-1783	463	16	8)	8)	NUM
eurjchem-1783	463	17	2.2.9	2.2.9	NUM
eurjchem-1783	463	18	.	.	PUNCT
eurjchem-1783	464	1	synthesis	synthesis	NOUN
eurjchem-1783	464	2	of	of	ADP
eurjchem-1783	464	3	tert	tert	NOUN
eurjchem-1783	464	4	-	-	PUNCT
eurjchem-1783	464	5	butyl	butyl	NOUN
eurjchem-1783	464	6	4-(4-(((benzyloxy	4-(4-(((benzyloxy	NOUN
eurjchem-1783	464	7	)	)	PUNCT
eurjchem-1783	464	8	carbonyl	carbonyl	NOUN
eurjchem-1783	464	9	)	)	PUNCT
eurjchem-1783	464	10	amino)-2	amino)-2	PROPN
eurjchem-1783	464	11	-	-	PUNCT
eurjchem-1783	464	12	fluorophenyl	fluorophenyl	NOUN
eurjchem-1783	464	13	)	)	PUNCT
eurjchem-1783	464	14	piperazine-1	piperazine-1	NOUN
eurjchem-1783	464	15	-	-	NOUN
eurjchem-1783	464	16	carboxylate	carboxylate	NOUN
eurjchem-1783	464	17	(	(	PUNCT
eurjchem-1783	464	18	9	9	NUM
eurjchem-1783	464	19	)	)	PUNCT
eurjchem-1783	464	20	2.2.10	2.2.10	NUM
eurjchem-1783	464	21	.	.	PUNCT
eurjchem-1783	465	1	synthesis	synthesis	NOUN
eurjchem-1783	465	2	of	of	ADP
eurjchem-1783	465	3	(	(	PUNCT
eurjchem-1783	465	4	r)-tert	r)-tert	ADJ
eurjchem-1783	465	5	-	-	PUNCT
eurjchem-1783	465	6	butyl	butyl	NOUN
eurjchem-1783	465	7	4-(4-(5-(bromomethyl)-2	4-(4-(5-(bromomethyl)-2	NOUN
eurjchem-1783	465	8	-	-	PUNCT
eurjchem-1783	465	9	oxooxazolidin-3	oxooxazolidin-3	NUM
eurjchem-1783	465	10	-	-	PUNCT
eurjchem-1783	465	11	yl)-2	yl)-2	NOUN
eurjchem-1783	465	12	-	-	PUNCT
eurjchem-1783	465	13	fluorophenyl	fluorophenyl	NOUN
eurjchem-1783	465	14	)	)	PUNCT
eurjchem-1783	465	15	piperazine-1	piperazine-1	NOUN
eurjchem-1783	465	16	-	-	NOUN
eurjchem-1783	465	17	carboxylate	carboxylate	NOUN
eurjchem-1783	465	18	(	(	PUNCT
eurjchem-1783	465	19	10	10	NUM
eurjchem-1783	465	20	)	)	PUNCT
eurjchem-1783	465	21	2.2.11	2.2.11	NUM
eurjchem-1783	465	22	.	.	PUNCT
eurjchem-1783	466	1	synthesis	synthesis	NOUN
eurjchem-1783	466	2	of	of	ADP
eurjchem-1783	466	3	(	(	PUNCT
eurjchem-1783	466	4	s)-tert	s)-tert	NOUN
eurjchem-1783	466	5	-	-	PUNCT
eurjchem-1783	466	6	butyl	butyl	NOUN
eurjchem-1783	466	7	4-(4-(5-(acetamido	4-(4-(5-(acetamido	NOUN
eurjchem-1783	466	8	methyl)-2	methyl)-2	NOUN
eurjchem-1783	466	9	-	-	PUNCT
eurjchem-1783	466	10	oxooxazolidin-3	oxooxazolidin-3	NUM
eurjchem-1783	466	11	-	-	PUNCT
eurjchem-1783	466	12	yl)-2	yl)-2	NOUN
eurjchem-1783	466	13	-	-	PUNCT
eurjchem-1783	466	14	fluorophenyl	fluorophenyl	NOUN
eurjchem-1783	466	15	)	)	PUNCT
eurjchem-1783	466	16	piperazine-1	piperazine-1	NOUN
eurjchem-1783	466	17	-	-	NOUN
eurjchem-1783	466	18	carboxylate	carboxylate	NOUN
eurjchem-1783	466	19	(	(	PUNCT
eurjchem-1783	466	20	11	11	NUM
eurjchem-1783	466	21	)	)	SYM
eurjchem-1783	466	22	2.2.12	2.2.12	NUM
eurjchem-1783	466	23	.	.	PUNCT
eurjchem-1783	467	1	synthesis	synthesis	NOUN
eurjchem-1783	467	2	of	of	ADP
eurjchem-1783	467	3	(	(	PUNCT
eurjchem-1783	467	4	s)-n-((3-(3	s)-n-((3-(3	PROPN
eurjchem-1783	467	5	-	-	PUNCT
eurjchem-1783	467	6	fluoro-4-(piperazin-1	fluoro-4-(piperazin-1	NOUN
eurjchem-1783	467	7	-	-	PUNCT
eurjchem-1783	467	8	yl	yl	NOUN
eurjchem-1783	467	9	)	)	PUNCT
eurjchem-1783	467	10	phenyl)-2	phenyl)-2	PROPN
eurjchem-1783	467	11	-	-	PUNCT
eurjchem-1783	467	12	oxooxazolidin-5	oxooxazolidin-5	NUM
eurjchem-1783	467	13	-	-	PUNCT
eurjchem-1783	467	14	yl	yl	NOUN
eurjchem-1783	467	15	)	)	PUNCT
eurjchem-1783	467	16	methyl	methyl	NOUN
eurjchem-1783	467	17	)	)	PUNCT
eurjchem-1783	467	18	acetamide	acetamide	NOUN
eurjchem-1783	467	19	(	(	PUNCT
eurjchem-1783	467	20	12	12	NUM
eurjchem-1783	467	21	)	)	PUNCT
eurjchem-1783	467	22	2.2.13	2.2.13	NUM
eurjchem-1783	467	23	.	.	PUNCT
eurjchem-1783	468	1	synthesis	synthesis	NOUN
eurjchem-1783	468	2	of	of	ADP
eurjchem-1783	468	3	(	(	PUNCT
eurjchem-1783	468	4	s)-n-((3-(3	s)-n-((3-(3	PROPN
eurjchem-1783	468	5	-	-	PUNCT
eurjchem-1783	468	6	fluoro-4-(4-(2	fluoro-4-(4-(2	NOUN
eurjchem-1783	468	7	-	-	PUNCT
eurjchem-1783	468	8	hydroxy	hydroxy	NOUN
eurjchem-1783	468	9	acetyl	acetyl	NOUN
eurjchem-1783	468	10	)	)	PUNCT
eurjchem-1783	468	11	piperazin-1	piperazin-1	PROPN
eurjchem-1783	468	12	-	-	PUNCT
eurjchem-1783	468	13	yl	yl	NOUN
eurjchem-1783	468	14	)	)	PUNCT
eurjchem-1783	468	15	phenyl)-2	phenyl)-2	PROPN
eurjchem-1783	468	16	-	-	PUNCT
eurjchem-1783	468	17	oxooxazolidin-5	oxooxazolidin-5	NUM
eurjchem-1783	468	18	-	-	PUNCT
eurjchem-1783	468	19	yl	yl	NOUN
eurjchem-1783	468	20	)	)	PUNCT
eurjchem-1783	468	21	methyl	methyl	NOUN
eurjchem-1783	468	22	)	)	PUNCT
eurjchem-1783	468	23	acetamide	acetamide	NOUN
eurjchem-1783	468	24	(	(	PUNCT
eurjchem-1783	468	25	13	13	NUM
eurjchem-1783	468	26	)	)	PUNCT
eurjchem-1783	468	27	3	3	NUM
eurjchem-1783	468	28	.	.	NOUN
eurjchem-1783	468	29	results	result	NOUN
eurjchem-1783	468	30	and	and	CCONJ
eurjchem-1783	468	31	discussion	discussion	NOUN
eurjchem-1783	468	32	4	4	NUM
eurjchem-1783	468	33	.	.	PUNCT
eurjchem-1783	469	1	conclusions	conclusion	NOUN
eurjchem-1783	469	2	disclosure	disclosure	NOUN
eurjchem-1783	469	3	statement	statement	NOUN
eurjchem-1783	469	4	orcid	orcid	PROPN
eurjchem-1783	469	5	references	reference	NOUN
eurjchem-1783	469	6	printfield10	printfield10	NOUN
eurjchem-1783	469	7	:	:	PUNCT
eurjchem-1783	469	8	printfield11	printfield11	NOUN
eurjchem-1783	469	9	:	:	PUNCT
eurjchem-1783	469	10	printfield12	printfield12	PROPN
eurjchem-1783	469	11	:	:	PUNCT
eurjchem-1783	469	12	printfield13	printfield13	VERB
eurjchem-1783	469	13	:	:	PUNCT
eurjchem-1783	469	14	printfield14	printfield14	NOUN
eurjchem-1783	469	15	:	:	PUNCT
eurjchem-1783	469	16	printfield15	printfield15	NOUN
eurjchem-1783	469	17	:	:	PUNCT
eurjchem-1783	469	18	printfield16	printfield16	ADJ
eurjchem-1783	469	19	:	:	PUNCT
eurjchem-1783	469	20	printfield20	printfield20	VERB
eurjchem-1783	469	21	:	:	PUNCT
eurjchem-1783	469	22	printfield21	printfield21	ADJ
eurjchem-1783	469	23	:	:	PUNCT
eurjchem-1783	469	24	printfield22	printfield22	NOUN
eurjchem-1783	469	25	:	:	PUNCT
eurjchem-1783	469	26	printfield23	printfield23	NOUN
eurjchem-1783	469	27	:	:	PUNCT
eurjchem-1783	469	28	printfield24	printfield24	NOUN
eurjchem-1783	469	29	:	:	PUNCT
eurjchem-1783	469	30	printfield25	printfield25	NOUN
eurjchem-1783	469	31	:	:	PUNCT
eurjchem-1783	469	32	printfield26	printfield26	ADJ
eurjchem-1783	469	33	:	:	PUNCT