id	sid	tid	token	lemma	pos
eurjchem-1922	1	1	synthesis	synthesis	NOUN
eurjchem-1922	1	2	,	,	PUNCT
eurjchem-1922	1	3	structural	structural	ADJ
eurjchem-1922	1	4	elucidation	elucidation	NOUN
eurjchem-1922	1	5	and	and	CCONJ
eurjchem-1922	1	6	x	x	NOUN
eurjchem-1922	1	7	-	-	NOUN
eurjchem-1922	1	8	ray	ray	NOUN
eurjchem-1922	1	9	crystallographic	crystallographic	ADJ
eurjchem-1922	1	10	studies	study	NOUN
eurjchem-1922	1	11	of	of	ADP
eurjchem-1922	1	12	1-(3,5	1-(3,5	NOUN
eurjchem-1922	1	13	-	-	PUNCT
eurjchem-1922	1	14	bis(trifluoromethyl)phenyl)-3-(dimethylamino)prop-2	bis(trifluoromethyl)phenyl)-3-(dimethylamino)prop-2	NOUN
eurjchem-1922	1	15	-	-	PUNCT
eurjchem-1922	1	16	en-1	en-1	NOUN
eurjchem-1922	1	17	-	-	PUNCT
eurjchem-1922	1	18	one	one	NUM
eurjchem-1922	1	19	european	european	ADJ
eurjchem-1922	1	20	journal	journal	NOUN
eurjchem-1922	1	21	of	of	ADP
eurjchem-1922	1	22	chemistry	chemistry	NOUN
eurjchem-1922	1	23	10	10	NUM
eurjchem-1922	1	24	(	(	PUNCT
eurjchem-1922	1	25	4	4	NUM
eurjchem-1922	1	26	)	)	PUNCT
eurjchem-1922	1	27	(	(	PUNCT
eurjchem-1922	1	28	2019	2019	NUM
eurjchem-1922	1	29	)	)	PUNCT
eurjchem-1922	1	30	381	381	NUM
eurjchem-1922	1	31	-	-	SYM
eurjchem-1922	1	32	385	385	NUM
eurjchem-1922	1	33	european	european	PROPN
eurjchem-1922	1	34	journal	journal	PROPN
eurjchem-1922	1	35	of	of	ADP
eurjchem-1922	1	36	chemistry	chemistry	NOUN
eurjchem-1922	1	37	view	view	NOUN
eurjchem-1922	1	38	journal	journal	PROPN
eurjchem-1922	1	39	online	online	PROPN
eurjchem-1922	1	40	view	view	NOUN
eurjchem-1922	1	41	article	article	NOUN
eurjchem-1922	1	42	online	online	ADJ
eurjchem-1922	1	43	synthesis	synthesis	NOUN
eurjchem-1922	1	44	,	,	PUNCT
eurjchem-1922	1	45	structural	structural	ADJ
eurjchem-1922	1	46	elucidation	elucidation	NOUN
eurjchem-1922	1	47	and	and	CCONJ
eurjchem-1922	1	48	x	x	NOUN
eurjchem-1922	1	49	-	-	NOUN
eurjchem-1922	1	50	ray	ray	NOUN
eurjchem-1922	1	51	crystallographic	crystallographic	ADJ
eurjchem-1922	1	52	studies	study	NOUN
eurjchem-1922	1	53	of	of	ADP
eurjchem-1922	1	54	1-(3,5	1-(3,5	NOUN
eurjchem-1922	1	55	-	-	PUNCT
eurjchem-1922	1	56	bis(trifluoromethyl)phenyl)-3-(dimethylamino)prop-2	bis(trifluoromethyl)phenyl)-3-(dimethylamino)prop-2	NOUN
eurjchem-1922	1	57	-	-	PUNCT
eurjchem-1922	1	58	en-1	en-1	NOUN
eurjchem-1922	1	59	-	-	PUNCT
eurjchem-1922	1	60	one	one	NUM
eurjchem-1922	1	61	stability	stability	NOUN
eurjchem-1922	1	62	nongrum	nongrum	NOUN
eurjchem-1922	1	63	,	,	PUNCT
eurjchem-1922	1	64	susma	susma	PROPN
eurjchem-1922	1	65	das	das	PROPN
eurjchem-1922	1	66	,	,	PUNCT
eurjchem-1922	1	67	shikpika	shikpika	NOUN
eurjchem-1922	1	68	khanikar	khanikar	NOUN
eurjchem-1922	1	69	and	and	CCONJ
eurjchem-1922	1	70	jai	jai	PROPN
eurjchem-1922	1	71	narain	narain	PROPN
eurjchem-1922	1	72	vishwakarma	vishwakarma	PROPN
eurjchem-1922	1	73	*	*	PUNCT
eurjchem-1922	1	74	organic	organic	ADJ
eurjchem-1922	1	75	research	research	NOUN
eurjchem-1922	1	76	laboratory	laboratory	NOUN
eurjchem-1922	1	77	,	,	PUNCT
eurjchem-1922	1	78	department	department	NOUN
eurjchem-1922	1	79	of	of	ADP
eurjchem-1922	1	80	chemical	chemical	PROPN
eurjchem-1922	1	81	science	science	PROPN
eurjchem-1922	1	82	,	,	PUNCT
eurjchem-1922	1	83	assam	assam	PROPN
eurjchem-1922	1	84	don	don	PROPN
eurjchem-1922	1	85	bosco	bosco	PROPN
eurjchem-1922	1	86	university	university	PROPN
eurjchem-1922	1	87	,	,	PUNCT
eurjchem-1922	1	88	tapesia	tapesia	PROPN
eurjchem-1922	1	89	gardens	gardens	PROPN
eurjchem-1922	1	90	,	,	PUNCT
eurjchem-1922	1	91	kamarkuchi	kamarkuchi	NOUN
eurjchem-1922	1	92	,	,	PUNCT
eurjchem-1922	1	93	sonapur	sonapur	NOUN
eurjchem-1922	1	94	,	,	PUNCT
eurjchem-1922	1	95	782	782	NUM
eurjchem-1922	1	96	402	402	NUM
eurjchem-1922	1	97	assam	assam	NOUN
eurjchem-1922	1	98	,	,	PUNCT
eurjchem-1922	1	99	india	india	PROPN
eurjchem-1922	1	100	stabilitynongrum@gmail.com	stabilitynongrum@gmail.com	PROPN
eurjchem-1922	1	101	(	(	PUNCT
eurjchem-1922	1	102	s.n	s.n	PROPN
eurjchem-1922	1	103	.	.	PROPN
eurjchem-1922	1	104	)	)	PUNCT
eurjchem-1922	1	105	,	,	PUNCT
eurjchem-1922	1	106	susmadas91@gmail.com	susmadas91@gmail.com	X
eurjchem-1922	1	107	(	(	PUNCT
eurjchem-1922	1	108	s.d	s.d	PROPN
eurjchem-1922	1	109	.	.	PROPN
eurjchem-1922	1	110	)	)	PUNCT
eurjchem-1922	1	111	,	,	PUNCT
eurjchem-1922	1	112	shilpikakhanikar11@gmail.com	shilpikakhanikar11@gmail.com	X
eurjchem-1922	1	113	(	(	PUNCT
eurjchem-1922	1	114	s.k	s.k	PROPN
eurjchem-1922	1	115	.	.	PROPN
eurjchem-1922	1	116	)	)	PUNCT
eurjchem-1922	1	117	,	,	PUNCT
eurjchem-1922	1	118	jnvishwakarma@rediffmail.com	jnvishwakarma@rediffmail.com	X
eurjchem-1922	1	119	(	(	PUNCT
eurjchem-1922	1	120	j.n.v	j.n.v	PROPN
eurjchem-1922	1	121	.	.	PUNCT
eurjchem-1922	1	122	)	)	PUNCT
eurjchem-1922	2	1	*	*	PUNCT
eurjchem-1922	2	2	corresponding	correspond	VERB
eurjchem-1922	2	3	author	author	NOUN
eurjchem-1922	2	4	at	at	ADP
eurjchem-1922	2	5	:	:	PUNCT
eurjchem-1922	2	6	organic	organic	ADJ
eurjchem-1922	2	7	research	research	NOUN
eurjchem-1922	2	8	laboratory	laboratory	NOUN
eurjchem-1922	2	9	,	,	PUNCT
eurjchem-1922	2	10	department	department	NOUN
eurjchem-1922	2	11	of	of	ADP
eurjchem-1922	2	12	chemical	chemical	PROPN
eurjchem-1922	2	13	science	science	PROPN
eurjchem-1922	2	14	,	,	PUNCT
eurjchem-1922	2	15	assam	assam	PROPN
eurjchem-1922	2	16	don	don	PROPN
eurjchem-1922	2	17	bosco	bosco	PROPN
eurjchem-1922	2	18	university	university	PROPN
eurjchem-1922	2	19	,	,	PUNCT
eurjchem-1922	2	20	tapesia	tapesia	PROPN
eurjchem-1922	2	21	gardens	gardens	PROPN
eurjchem-1922	2	22	,	,	PUNCT
eurjchem-1922	2	23	kamarkuchi	kamarkuchi	NOUN
eurjchem-1922	2	24	,	,	PUNCT
eurjchem-1922	2	25	sonapur	sonapur	NOUN
eurjchem-1922	2	26	,	,	PUNCT
eurjchem-1922	2	27	782	782	NUM
eurjchem-1922	2	28	402	402	NUM
eurjchem-1922	2	29	assam	assam	PROPN
eurjchem-1922	2	30	,	,	PUNCT
eurjchem-1922	2	31	india	india	PROPN
eurjchem-1922	2	32	.	.	PUNCT
eurjchem-1922	3	1	tel	tel	ADP
eurjchem-1922	3	2	:	:	PUNCT
eurjchem-1922	3	3	+91.91270.51222	+91.91270.51222	NOUN
eurjchem-1922	3	4	fax	fax	NOUN
eurjchem-1922	3	5	:	:	PUNCT
eurjchem-1922	3	6	+91.91270.51222	+91.91270.51222	NOUN
eurjchem-1922	3	7	e	e	NOUN
eurjchem-1922	3	8	-	-	NOUN
eurjchem-1922	3	9	mail	mail	NOUN
eurjchem-1922	3	10	:	:	PUNCT
eurjchem-1922	4	1	jnvishwakarma@rediffmail.com	jnvishwakarma@rediffmail.com	X
eurjchem-1922	4	2	(	(	PUNCT
eurjchem-1922	4	3	j.n	j.n	PROPN
eurjchem-1922	4	4	.	.	PROPN
eurjchem-1922	4	5	vishwakarma	vishwakarma	PROPN
eurjchem-1922	4	6	)	)	PUNCT
eurjchem-1922	4	7	.	.	PUNCT
eurjchem-1922	5	1	10.5155	10.5155	NUM
eurjchem-1922	5	2	/	/	SYM
eurjchem-1922	5	3	eurjchem.10.4.381	eurjchem.10.4.381	NOUN
eurjchem-1922	5	4	-	-	PUNCT
eurjchem-1922	5	5	385.1922	385.1922	NUM
eurjchem-1922	5	6	received	receive	VERB
eurjchem-1922	5	7	:	:	PUNCT
eurjchem-1922	5	8	03	03	NUM
eurjchem-1922	5	9	september	september	PROPN
eurjchem-1922	5	10	2019	2019	NUM
eurjchem-1922	5	11	received	receive	VERB
eurjchem-1922	5	12	in	in	ADP
eurjchem-1922	5	13	revised	revise	VERB
eurjchem-1922	5	14	form	form	NOUN
eurjchem-1922	5	15	:	:	PUNCT
eurjchem-1922	5	16	24	24	NUM
eurjchem-1922	5	17	september	september	PROPN
eurjchem-1922	5	18	2019	2019	NUM
eurjchem-1922	5	19	accepted	accept	VERB
eurjchem-1922	5	20	:	:	PUNCT
eurjchem-1922	5	21	06	06	NUM
eurjchem-1922	5	22	october	october	NOUN
eurjchem-1922	5	23	2019	2019	NUM
eurjchem-1922	5	24	published	publish	VERB
eurjchem-1922	5	25	online	online	ADV
eurjchem-1922	5	26	:	:	PUNCT
eurjchem-1922	5	27	31	31	NUM
eurjchem-1922	5	28	december	december	PROPN
eurjchem-1922	5	29	2019	2019	NUM
eurjchem-1922	5	30	printed	print	VERB
eurjchem-1922	5	31	:	:	PUNCT
eurjchem-1922	5	32	31	31	NUM
eurjchem-1922	5	33	december	december	PROPN
eurjchem-1922	5	34	2019	2019	NUM
eurjchem-1922	5	35	a	a	DET
eurjchem-1922	5	36	new	new	ADJ
eurjchem-1922	5	37	enaminone	enaminone	NOUN
eurjchem-1922	5	38	was	be	AUX
eurjchem-1922	5	39	synthesized	synthesize	VERB
eurjchem-1922	5	40	by	by	ADP
eurjchem-1922	5	41	reacting	react	VERB
eurjchem-1922	5	42	3,5	3,5	NUM
eurjchem-1922	5	43	-	-	PUNCT
eurjchem-1922	5	44	bis-(trifluoromethyl)acetophenones	bis-(trifluoromethyl)acetophenone	NOUN
eurjchem-1922	5	45	and	and	CCONJ
eurjchem-1922	5	46	n	n	CCONJ
eurjchem-1922	5	47	,	,	PUNCT
eurjchem-1922	5	48	n	n	CCONJ
eurjchem-1922	5	49	-	-	PUNCT
eurjchem-1922	5	50	dimethylformamide	dimethylformamide	NOUN
eurjchem-1922	5	51	dimethyl	dimethyl	NOUN
eurjchem-1922	5	52	acetal	acetal	NOUN
eurjchem-1922	5	53	and	and	CCONJ
eurjchem-1922	5	54	its	its	PRON
eurjchem-1922	5	55	detailed	detailed	ADJ
eurjchem-1922	5	56	structural	structural	ADJ
eurjchem-1922	5	57	and	and	CCONJ
eurjchem-1922	5	58	crystalline	crystalline	NOUN
eurjchem-1922	5	59	properties	property	NOUN
eurjchem-1922	5	60	were	be	AUX
eurjchem-1922	5	61	studied	study	VERB
eurjchem-1922	5	62	.	.	PUNCT
eurjchem-1922	6	1	the	the	DET
eurjchem-1922	6	2	crystal	crystal	PROPN
eurjchem-1922	6	3	data	datum	NOUN
eurjchem-1922	6	4	were	be	AUX
eurjchem-1922	6	5	found	find	VERB
eurjchem-1922	6	6	to	to	PART
eurjchem-1922	6	7	be	be	AUX
eurjchem-1922	6	8	as	as	ADP
eurjchem-1922	6	9	c13h11f6no	c13h11f6no	VERB
eurjchem-1922	6	10	,	,	PUNCT
eurjchem-1922	6	11	monoclinic	monoclinic	ADJ
eurjchem-1922	6	12	,	,	PUNCT
eurjchem-1922	6	13	space	space	NOUN
eurjchem-1922	6	14	group	group	NOUN
eurjchem-1922	6	15	p21	p21	PROPN
eurjchem-1922	6	16	/	/	SYM
eurjchem-1922	6	17	c	c	PROPN
eurjchem-1922	6	18	(	(	PUNCT
eurjchem-1922	6	19	no	no	INTJ
eurjchem-1922	6	20	.	.	NOUN
eurjchem-1922	6	21	14	14	NUM
eurjchem-1922	6	22	)	)	PUNCT
eurjchem-1922	6	23	,	,	PUNCT
eurjchem-1922	6	24	a	a	DET
eurjchem-1922	6	25	=	=	SYM
eurjchem-1922	6	26	8.1556(8	8.1556(8	NOUN
eurjchem-1922	6	27	)	)	PUNCT
eurjchem-1922	6	28	å	å	PROPN
eurjchem-1922	6	29	,	,	PUNCT
eurjchem-1922	6	30	b	b	X
eurjchem-1922	6	31	=	=	SYM
eurjchem-1922	6	32	24.877(3	24.877(3	PROPN
eurjchem-1922	6	33	)	)	PUNCT
eurjchem-1922	6	34	å	å	NOUN
eurjchem-1922	6	35	,	,	PUNCT
eurjchem-1922	6	36	c	c	NOUN
eurjchem-1922	6	37	=	=	SYM
eurjchem-1922	6	38	7.6067(7	7.6067(7	NUM
eurjchem-1922	6	39	)	)	PUNCT
eurjchem-1922	7	1	å	å	NOUN
eurjchem-1922	7	2	,	,	PUNCT
eurjchem-1922	7	3	β	β	X
eurjchem-1922	7	4	=	=	SYM
eurjchem-1922	7	5	116.745(6	116.745(6	PROPN
eurjchem-1922	7	6	)	)	PUNCT
eurjchem-1922	7	7	°	°	NOUN
eurjchem-1922	7	8	,	,	PUNCT
eurjchem-1922	7	9	v	v	NOUN
eurjchem-1922	7	10	=	=	SYM
eurjchem-1922	7	11	1378.2(3	1378.2(3	X
eurjchem-1922	7	12	)	)	PUNCT
eurjchem-1922	7	13	å3	å3	PROPN
eurjchem-1922	7	14	,	,	PUNCT
eurjchem-1922	7	15	z	z	NOUN
eurjchem-1922	7	16	=	=	SYM
eurjchem-1922	7	17	4	4	NUM
eurjchem-1922	7	18	,	,	PUNCT
eurjchem-1922	7	19	t	t	NOUN
eurjchem-1922	7	20	=	=	SYM
eurjchem-1922	7	21	293(2	293(2	NUM
eurjchem-1922	7	22	)	)	PUNCT
eurjchem-1922	7	23	k	k	NOUN
eurjchem-1922	7	24	,	,	PUNCT
eurjchem-1922	7	25	μ(mokα	μ(mokα	NOUN
eurjchem-1922	7	26	)	)	PUNCT
eurjchem-1922	7	27	=	=	SYM
eurjchem-1922	8	1	0.150	0.150	NUM
eurjchem-1922	8	2	mm-1	mm-1	NOUN
eurjchem-1922	8	3	,	,	PUNCT
eurjchem-1922	8	4	dcalc	dcalc	NOUN
eurjchem-1922	8	5	=	=	NOUN
eurjchem-1922	8	6	1.500	1.500	NUM
eurjchem-1922	8	7	g	g	NOUN
eurjchem-1922	8	8	/	/	SYM
eurjchem-1922	8	9	cm3	cm3	NOUN
eurjchem-1922	8	10	,	,	PUNCT
eurjchem-1922	8	11	40777	40777	NUM
eurjchem-1922	8	12	reflections	reflection	NOUN
eurjchem-1922	8	13	measured	measure	VERB
eurjchem-1922	8	14	(	(	PUNCT
eurjchem-1922	8	15	5.594	5.594	NUM
eurjchem-1922	8	16	°	°	NOUN
eurjchem-1922	8	17	≤	≤	NUM
eurjchem-1922	8	18	2θ	2θ	NUM
eurjchem-1922	8	19	≤	≤	NUM
eurjchem-1922	8	20	56.786	56.786	NUM
eurjchem-1922	8	21	°	°	NUM
eurjchem-1922	8	22	)	)	PUNCT
eurjchem-1922	8	23	,	,	PUNCT
eurjchem-1922	8	24	3413	3413	NUM
eurjchem-1922	8	25	unique	unique	ADJ
eurjchem-1922	8	26	(	(	PUNCT
eurjchem-1922	8	27	rint	rint	NOUN
eurjchem-1922	8	28	=	=	SYM
eurjchem-1922	8	29	0.1040	0.1040	NUM
eurjchem-1922	8	30	,	,	PUNCT
eurjchem-1922	8	31	rsigma	rsigma	ADJ
eurjchem-1922	8	32	=	=	SYM
eurjchem-1922	8	33	0.0584	0.0584	NUM
eurjchem-1922	8	34	)	)	PUNCT
eurjchem-1922	8	35	which	which	PRON
eurjchem-1922	8	36	were	be	AUX
eurjchem-1922	8	37	used	use	VERB
eurjchem-1922	8	38	in	in	ADP
eurjchem-1922	8	39	all	all	DET
eurjchem-1922	8	40	calculations	calculation	NOUN
eurjchem-1922	8	41	.	.	PUNCT
eurjchem-1922	9	1	the	the	DET
eurjchem-1922	9	2	final	final	ADJ
eurjchem-1922	9	3	r1	r1	NOUN
eurjchem-1922	9	4	was	be	AUX
eurjchem-1922	9	5	0.0771	0.0771	NUM
eurjchem-1922	9	6	(	(	PUNCT
eurjchem-1922	9	7	i	i	X
eurjchem-1922	9	8	>	>	X
eurjchem-1922	9	9	2σ(i	2σ(i	NUM
eurjchem-1922	9	10	)	)	PUNCT
eurjchem-1922	9	11	)	)	PUNCT
eurjchem-1922	10	1	and	and	CCONJ
eurjchem-1922	10	2	wr2	wr2	PROPN
eurjchem-1922	10	3	was	be	AUX
eurjchem-1922	10	4	0.2541	0.2541	NUM
eurjchem-1922	10	5	(	(	PUNCT
eurjchem-1922	10	6	all	all	DET
eurjchem-1922	10	7	data	datum	NOUN
eurjchem-1922	10	8	)	)	PUNCT
eurjchem-1922	10	9	.	.	PUNCT
eurjchem-1922	11	1	enaminones	enaminone	NOUN
eurjchem-1922	11	2	acetophenone	acetophenone	PROPN
eurjchem-1922	11	3	trifluoromethyl	trifluoromethyl	NOUN
eurjchem-1922	11	4	x	x	PROPN
eurjchem-1922	11	5	-	-	NOUN
eurjchem-1922	11	6	ray	ray	NOUN
eurjchem-1922	11	7	crystallography	crystallography	NOUN
eurjchem-1922	11	8	geometric	geometric	ADJ
eurjchem-1922	11	9	parameters	parameter	NOUN
eurjchem-1922	11	10	n	n	CCONJ
eurjchem-1922	11	11	,	,	PUNCT
eurjchem-1922	11	12	n	n	CCONJ
eurjchem-1922	11	13	-	-	PUNCT
eurjchem-1922	11	14	dimethylformamide	dimethylformamide	NOUN
eurjchem-1922	11	15	dimethyl	dimethyl	NOUN
eurjchem-1922	11	16	acetal	acetal	NOUN
eurjchem-1922	11	17	cite	cite	VERB
eurjchem-1922	11	18	this	this	PRON
eurjchem-1922	11	19	:	:	PUNCT
eurjchem-1922	11	20	eur	eur	PROPN
eurjchem-1922	11	21	.	.	PUNCT
eurjchem-1922	12	1	j.	j.	PROPN
eurjchem-1922	12	2	chem	chem	PROPN
eurjchem-1922	12	3	.	.	PUNCT
eurjchem-1922	13	1	2019	2019	NUM
eurjchem-1922	13	2	,	,	PUNCT
eurjchem-1922	13	3	10(4	10(4	NUM
eurjchem-1922	13	4	)	)	PUNCT
eurjchem-1922	13	5	,	,	PUNCT
eurjchem-1922	13	6	381	381	NUM
eurjchem-1922	13	7	-	-	SYM
eurjchem-1922	13	8	385	385	NUM
eurjchem-1922	13	9	journal	journal	NOUN
eurjchem-1922	13	10	website	website	NOUN
eurjchem-1922	13	11	:	:	PUNCT
eurjchem-1922	13	12	www.eurjchem.com	www.eurjchem.com	X
eurjchem-1922	13	13	1	1	X
eurjchem-1922	13	14	.	.	PUNCT
eurjchem-1922	13	15	introduction	introduction	NOUN
eurjchem-1922	13	16	fluorine	fluorine	NOUN
eurjchem-1922	13	17	containing	contain	VERB
eurjchem-1922	13	18	naturally	naturally	ADV
eurjchem-1922	13	19	occurring	occur	VERB
eurjchem-1922	13	20	compounds	compound	NOUN
eurjchem-1922	13	21	are	be	AUX
eurjchem-1922	13	22	very	very	ADV
eurjchem-1922	13	23	few	few	ADJ
eurjchem-1922	13	24	to	to	PART
eurjchem-1922	13	25	be	be	AUX
eurjchem-1922	13	26	found	find	VERB
eurjchem-1922	13	27	[	[	X
eurjchem-1922	13	28	1	1	NUM
eurjchem-1922	13	29	]	]	PUNCT
eurjchem-1922	13	30	,	,	PUNCT
eurjchem-1922	13	31	however	however	ADV
eurjchem-1922	13	32	,	,	PUNCT
eurjchem-1922	13	33	about	about	ADV
eurjchem-1922	13	34	25	25	NUM
eurjchem-1922	13	35	%	%	NOUN
eurjchem-1922	13	36	of	of	ADP
eurjchem-1922	13	37	the	the	DET
eurjchem-1922	13	38	marketed	market	VERB
eurjchem-1922	13	39	drug	drug	NOUN
eurjchem-1922	13	40	molecules	molecule	NOUN
eurjchem-1922	13	41	are	be	AUX
eurjchem-1922	13	42	embedded	embed	VERB
eurjchem-1922	13	43	with	with	ADP
eurjchem-1922	13	44	fluorine	fluorine	NOUN
eurjchem-1922	13	45	atoms	atom	NOUN
eurjchem-1922	13	46	[	[	X
eurjchem-1922	13	47	2	2	NUM
eurjchem-1922	13	48	]	]	PUNCT
eurjchem-1922	13	49	.	.	PUNCT
eurjchem-1922	14	1	fluorine	fluorine	NOUN
eurjchem-1922	14	2	,	,	PUNCT
eurjchem-1922	14	3	the	the	DET
eurjchem-1922	14	4	most	most	ADV
eurjchem-1922	14	5	electronegative	electronegative	ADJ
eurjchem-1922	14	6	element	element	NOUN
eurjchem-1922	14	7	in	in	ADP
eurjchem-1922	14	8	periodic	periodic	ADJ
eurjchem-1922	14	9	table	table	NOUN
eurjchem-1922	14	10	and	and	CCONJ
eurjchem-1922	14	11	also	also	ADV
eurjchem-1922	14	12	capable	capable	ADJ
eurjchem-1922	14	13	of	of	ADP
eurjchem-1922	14	14	forming	form	VERB
eurjchem-1922	14	15	hydrogen	hydrogen	NOUN
eurjchem-1922	14	16	-	-	PUNCT
eurjchem-1922	14	17	bond	bond	NOUN
eurjchem-1922	14	18	,	,	PUNCT
eurjchem-1922	14	19	can	can	AUX
eurjchem-1922	14	20	induce	induce	VERB
eurjchem-1922	14	21	a	a	DET
eurjchem-1922	14	22	strong	strong	ADJ
eurjchem-1922	14	23	plorization	plorization	NOUN
eurjchem-1922	14	24	on	on	ADP
eurjchem-1922	14	25	its	its	PRON
eurjchem-1922	14	26	neighbouring	neighbouring	ADJ
eurjchem-1922	14	27	elements	element	NOUN
eurjchem-1922	14	28	[	[	X
eurjchem-1922	14	29	1	1	NUM
eurjchem-1922	14	30	]	]	PUNCT
eurjchem-1922	14	31	.	.	PUNCT
eurjchem-1922	15	1	hence	hence	ADV
eurjchem-1922	15	2	,	,	PUNCT
eurjchem-1922	15	3	the	the	DET
eurjchem-1922	15	4	presence	presence	NOUN
eurjchem-1922	15	5	of	of	ADP
eurjchem-1922	15	6	fluorinated	fluorinate	VERB
eurjchem-1922	15	7	groups	group	NOUN
eurjchem-1922	15	8	in	in	ADP
eurjchem-1922	15	9	biologically	biologically	ADV
eurjchem-1922	15	10	active	active	ADJ
eurjchem-1922	15	11	molecular	molecular	ADJ
eurjchem-1922	15	12	architectures	architecture	NOUN
eurjchem-1922	15	13	should	should	AUX
eurjchem-1922	15	14	influence	influence	VERB
eurjchem-1922	15	15	the	the	DET
eurjchem-1922	15	16	electronic	electronic	ADJ
eurjchem-1922	15	17	and	and	CCONJ
eurjchem-1922	15	18	binding	bind	VERB
eurjchem-1922	15	19	properties	property	NOUN
eurjchem-1922	15	20	,	,	PUNCT
eurjchem-1922	15	21	metabolic	metabolic	NOUN
eurjchem-1922	15	22	stability	stability	NOUN
eurjchem-1922	15	23	and	and	CCONJ
eurjchem-1922	15	24	lipophilicity	lipophilicity	NOUN
eurjchem-1922	15	25	enhancing	enhance	VERB
eurjchem-1922	15	26	the	the	DET
eurjchem-1922	15	27	drug	drug	NOUN
eurjchem-1922	15	28	optimization	optimization	NOUN
eurjchem-1922	15	29	capablities	capablitie	NOUN
eurjchem-1922	15	30	of	of	ADP
eurjchem-1922	15	31	a	a	DET
eurjchem-1922	15	32	lead	lead	ADJ
eurjchem-1922	15	33	molecule	molecule	NOUN
eurjchem-1922	15	34	.	.	PUNCT
eurjchem-1922	16	1	trifluoromethylated	trifluoromethylate	VERB
eurjchem-1922	16	2	alkenes	alkene	NOUN
eurjchem-1922	16	3	are	be	AUX
eurjchem-1922	16	4	considered	consider	VERB
eurjchem-1922	16	5	very	very	ADV
eurjchem-1922	16	6	important	important	ADJ
eurjchem-1922	16	7	pharmacophores	pharmacophore	NOUN
eurjchem-1922	16	8	and	and	CCONJ
eurjchem-1922	16	9	have	have	AUX
eurjchem-1922	16	10	been	be	AUX
eurjchem-1922	16	11	gaining	gain	VERB
eurjchem-1922	16	12	propularity	propularity	NOUN
eurjchem-1922	16	13	in	in	ADP
eurjchem-1922	16	14	pharmaceuticals	pharmaceutical	NOUN
eurjchem-1922	16	15	and	and	CCONJ
eurjchem-1922	16	16	agro	agro	NOUN
eurjchem-1922	16	17	-	-	PUNCT
eurjchem-1922	16	18	sciences	science	NOUN
eurjchem-1922	16	19	[	[	X
eurjchem-1922	16	20	3	3	NUM
eurjchem-1922	16	21	]	]	PUNCT
eurjchem-1922	16	22	.	.	PUNCT
eurjchem-1922	17	1	a	a	DET
eurjchem-1922	17	2	number	number	NOUN
eurjchem-1922	17	3	of	of	ADP
eurjchem-1922	17	4	fluorine	fluorine	NOUN
eurjchem-1922	17	5	substituted	substitute	VERB
eurjchem-1922	17	6	drugs	drug	NOUN
eurjchem-1922	17	7	are	be	AUX
eurjchem-1922	17	8	available	available	ADJ
eurjchem-1922	17	9	in	in	ADP
eurjchem-1922	17	10	the	the	DET
eurjchem-1922	17	11	market	market	NOUN
eurjchem-1922	17	12	,	,	PUNCT
eurjchem-1922	17	13	which	which	PRON
eurjchem-1922	17	14	are	be	AUX
eurjchem-1922	17	15	prescribed	prescribe	VERB
eurjchem-1922	17	16	to	to	PART
eurjchem-1922	17	17	cure	cure	VERB
eurjchem-1922	17	18	a	a	DET
eurjchem-1922	17	19	wide	wide	ADJ
eurjchem-1922	17	20	range	range	NOUN
eurjchem-1922	17	21	of	of	ADP
eurjchem-1922	17	22	diseases	disease	NOUN
eurjchem-1922	17	23	[	[	X
eurjchem-1922	17	24	4	4	NUM
eurjchem-1922	17	25	]	]	PUNCT
eurjchem-1922	17	26	.	.	PUNCT
eurjchem-1922	18	1	encouraged	encourage	VERB
eurjchem-1922	18	2	by	by	ADP
eurjchem-1922	18	3	these	these	DET
eurjchem-1922	18	4	advantages	advantage	NOUN
eurjchem-1922	18	5	,	,	PUNCT
eurjchem-1922	18	6	a	a	DET
eurjchem-1922	18	7	good	good	ADJ
eurjchem-1922	18	8	degree	degree	NOUN
eurjchem-1922	18	9	of	of	ADP
eurjchem-1922	18	10	attention	attention	NOUN
eurjchem-1922	18	11	has	have	AUX
eurjchem-1922	18	12	been	be	AUX
eurjchem-1922	18	13	invested	invest	VERB
eurjchem-1922	18	14	towards	towards	ADP
eurjchem-1922	18	15	the	the	DET
eurjchem-1922	18	16	development	development	NOUN
eurjchem-1922	18	17	of	of	ADP
eurjchem-1922	18	18	newer	new	ADJ
eurjchem-1922	18	19	synthetic	synthetic	ADJ
eurjchem-1922	18	20	strategies	strategy	NOUN
eurjchem-1922	18	21	for	for	ADP
eurjchem-1922	18	22	mono-	mono-	NUM
eurjchem-1922	18	23	,	,	PUNCT
eurjchem-1922	18	24	diand	diand	NOUN
eurjchem-1922	18	25	tri	tri	VERB
eurjchem-1922	18	26	-	-	ADJ
eurjchem-1922	18	27	fluorinated	fluorinate	VERB
eurjchem-1922	18	28	molecular	molecular	ADJ
eurjchem-1922	18	29	entities	entity	NOUN
eurjchem-1922	18	30	[	[	X
eurjchem-1922	18	31	5,6	5,6	NUM
eurjchem-1922	18	32	]	]	X
eurjchem-1922	18	33	.	.	PUNCT
eurjchem-1922	19	1	literature	literature	NOUN
eurjchem-1922	19	2	reveals	reveal	VERB
eurjchem-1922	19	3	that	that	SCONJ
eurjchem-1922	19	4	enaminones	enaminone	NOUN
eurjchem-1922	19	5	are	be	AUX
eurjchem-1922	19	6	very	very	ADV
eurjchem-1922	19	7	versatile	versatile	ADJ
eurjchem-1922	19	8	predecessors	predecessor	NOUN
eurjchem-1922	19	9	for	for	ADP
eurjchem-1922	19	10	synthesizing	synthesize	VERB
eurjchem-1922	19	11	novel	novel	ADJ
eurjchem-1922	19	12	heterocyclic	heterocyclic	ADJ
eurjchem-1922	19	13	systems	system	NOUN
eurjchem-1922	19	14	as	as	SCONJ
eurjchem-1922	19	15	they	they	PRON
eurjchem-1922	19	16	can	can	AUX
eurjchem-1922	19	17	react	react	VERB
eurjchem-1922	19	18	with	with	ADP
eurjchem-1922	19	19	both	both	CCONJ
eurjchem-1922	19	20	electrophiles	electrophile	NOUN
eurjchem-1922	19	21	and	and	CCONJ
eurjchem-1922	19	22	nucleophiles	nucleophile	NOUN
eurjchem-1922	20	1	[	[	X
eurjchem-1922	20	2	7,8	7,8	NUM
eurjchem-1922	20	3	]	]	PUNCT
eurjchem-1922	20	4	.	.	PUNCT
eurjchem-1922	21	1	they	they	PRON
eurjchem-1922	21	2	also	also	ADV
eurjchem-1922	21	3	process	process	VERB
eurjchem-1922	21	4	many	many	ADJ
eurjchem-1922	21	5	biological	biological	ADJ
eurjchem-1922	21	6	properties	property	NOUN
eurjchem-1922	21	7	like	like	ADP
eurjchem-1922	21	8	antitumor	antitumor	PROPN
eurjchem-1922	21	9	,	,	PUNCT
eurjchem-1922	21	10	antimicrobial	antimicrobial	ADJ
eurjchem-1922	21	11	,	,	PUNCT
eurjchem-1922	21	12	anti	anti	ADJ
eurjchem-1922	21	13	-	-	ADJ
eurjchem-1922	21	14	inflammatory	inflammatory	ADJ
eurjchem-1922	21	15	,	,	PUNCT
eurjchem-1922	21	16	analgesic	analgesic	ADJ
eurjchem-1922	21	17	,	,	PUNCT
eurjchem-1922	21	18	ulcerogenic	ulcerogenic	ADJ
eurjchem-1922	21	19	agents	agent	NOUN
eurjchem-1922	21	20	[	[	X
eurjchem-1922	21	21	7	7	NUM
eurjchem-1922	21	22	]	]	PUNCT
eurjchem-1922	21	23	.	.	PUNCT
eurjchem-1922	22	1	promoted	promote	VERB
eurjchem-1922	22	2	by	by	ADP
eurjchem-1922	22	3	these	these	DET
eurjchem-1922	22	4	observations	observation	NOUN
eurjchem-1922	22	5	and	and	CCONJ
eurjchem-1922	22	6	in	in	ADP
eurjchem-1922	22	7	continuation	continuation	NOUN
eurjchem-1922	22	8	with	with	ADP
eurjchem-1922	22	9	our	our	PRON
eurjchem-1922	22	10	earlier	early	ADJ
eurjchem-1922	22	11	studies	study	NOUN
eurjchem-1922	22	12	on	on	ADP
eurjchem-1922	22	13	enaminones	enaminone	NOUN
eurjchem-1922	22	14	[	[	X
eurjchem-1922	22	15	9,10	9,10	NUM
eurjchem-1922	22	16	]	]	PUNCT
eurjchem-1922	22	17	,	,	PUNCT
eurjchem-1922	22	18	we	we	PRON
eurjchem-1922	22	19	decided	decide	VERB
eurjchem-1922	22	20	to	to	PART
eurjchem-1922	22	21	synthesise	synthesise	VERB
eurjchem-1922	22	22	the	the	DET
eurjchem-1922	22	23	title	title	NOUN
eurjchem-1922	22	24	compound	compound	NOUN
eurjchem-1922	22	25	,	,	PUNCT
eurjchem-1922	22	26	the	the	DET
eurjchem-1922	22	27	results	result	NOUN
eurjchem-1922	22	28	of	of	ADP
eurjchem-1922	22	29	which	which	PRON
eurjchem-1922	22	30	are	be	AUX
eurjchem-1922	22	31	presented	present	VERB
eurjchem-1922	22	32	herein	herein	NOUN
eurjchem-1922	22	33	(	(	PUNCT
eurjchem-1922	22	34	scheme	scheme	NOUN
eurjchem-1922	22	35	1	1	NUM
eurjchem-1922	22	36	)	)	PUNCT
eurjchem-1922	22	37	.	.	PUNCT
eurjchem-1922	23	1	2	2	X
eurjchem-1922	23	2	.	.	X
eurjchem-1922	23	3	experimental	experimental	ADJ
eurjchem-1922	23	4	2.1	2.1	NUM
eurjchem-1922	23	5	.	.	PUNCT
eurjchem-1922	24	1	instrumentation	instrumentation	NOUN
eurjchem-1922	24	2	1h	1h	NUM
eurjchem-1922	24	3	nmr	nmr	NOUN
eurjchem-1922	24	4	(	(	PUNCT
eurjchem-1922	24	5	300	300	NUM
eurjchem-1922	24	6	mhz	mhz	NOUN
eurjchem-1922	24	7	)	)	PUNCT
eurjchem-1922	24	8	and	and	CCONJ
eurjchem-1922	24	9	13c	13c	NOUN
eurjchem-1922	24	10	nmr	nmr	NOUN
eurjchem-1922	24	11	(	(	PUNCT
eurjchem-1922	24	12	75	75	NUM
eurjchem-1922	24	13	mhz	mhz	NOUN
eurjchem-1922	24	14	)	)	PUNCT
eurjchem-1922	24	15	were	be	AUX
eurjchem-1922	24	16	recorded	record	VERB
eurjchem-1922	24	17	on	on	ADP
eurjchem-1922	24	18	bruker	bruker	PROPN
eurjchem-1922	24	19	av	av	PROPN
eurjchem-1922	24	20	ii	ii	PROPN
eurjchem-1922	24	21	300	300	NUM
eurjchem-1922	24	22	mhz	mhz	NOUN
eurjchem-1922	24	23	.	.	PUNCT
eurjchem-1922	25	1	the	the	DET
eurjchem-1922	25	2	chemical	chemical	NOUN
eurjchem-1922	25	3	shift	shift	NOUN
eurjchem-1922	25	4	(	(	PUNCT
eurjchem-1922	25	5	δ	δ	NOUN
eurjchem-1922	25	6	ppm	ppm	PROPN
eurjchem-1922	25	7	)	)	PUNCT
eurjchem-1922	25	8	and	and	CCONJ
eurjchem-1922	25	9	the	the	DET
eurjchem-1922	25	10	coupling	coupling	NOUN
eurjchem-1922	25	11	constants	constant	NOUN
eurjchem-1922	25	12	(	(	PUNCT
eurjchem-1922	25	13	hz	hz	NOUN
eurjchem-1922	25	14	)	)	PUNCT
eurjchem-1922	25	15	are	be	AUX
eurjchem-1922	25	16	reported	report	VERB
eurjchem-1922	25	17	in	in	ADP
eurjchem-1922	25	18	the	the	DET
eurjchem-1922	25	19	standard	standard	ADJ
eurjchem-1922	25	20	fashion	fashion	NOUN
eurjchem-1922	25	21	with	with	ADP
eurjchem-1922	25	22	reference	reference	NOUN
eurjchem-1922	25	23	to	to	ADP
eurjchem-1922	25	24	tms	tms	PROPN
eurjchem-1922	25	25	as	as	ADP
eurjchem-1922	25	26	standard	standard	NOUN
eurjchem-1922	25	27	in	in	ADP
eurjchem-1922	25	28	cdcl3	cdcl3	PROPN
eurjchem-1922	25	29	.	.	PUNCT
eurjchem-1922	26	1	the	the	DET
eurjchem-1922	26	2	ft	ft	PROPN
eurjchem-1922	26	3	-	-	PUNCT
eurjchem-1922	26	4	ir	ir	PROPN
eurjchem-1922	26	5	spectra	spectra	NOUN
eurjchem-1922	26	6	were	be	AUX
eurjchem-1922	26	7	recorded	record	VERB
eurjchem-1922	26	8	on	on	ADP
eurjchem-1922	26	9	perkin	perkin	PROPN
eurjchem-1922	26	10	elmer	elmer	PROPN
eurjchem-1922	26	11	spectrum	spectrum	PROPN
eurjchem-1922	26	12	ii	ii	PROPN
eurjchem-1922	26	13	spectrophotometer	spectrophotometer	NOUN
eurjchem-1922	26	14	.	.	PUNCT
eurjchem-1922	27	1	the	the	DET
eurjchem-1922	27	2	melting	melting	NOUN
eurjchem-1922	27	3	point	point	NOUN
eurjchem-1922	27	4	was	be	AUX
eurjchem-1922	27	5	recorded	record	VERB
eurjchem-1922	27	6	using	use	VERB
eurjchem-1922	27	7	open	open	ADJ
eurjchem-1922	27	8	capillary	capillary	ADJ
eurjchem-1922	27	9	method	method	NOUN
eurjchem-1922	27	10	and	and	CCONJ
eurjchem-1922	27	11	is	be	AUX
eurjchem-1922	27	12	uncorrected	uncorrecte	VERB
eurjchem-1922	27	13	.	.	PUNCT
eurjchem-1922	28	1	x	x	X
eurjchem-1922	28	2	-	-	PUNCT
eurjchem-1922	28	3	ray	ray	NOUN
eurjchem-1922	28	4	diffraction	diffraction	NOUN
eurjchem-1922	28	5	data	datum	NOUN
eurjchem-1922	28	6	of	of	ADP
eurjchem-1922	28	7	the	the	DET
eurjchem-1922	28	8	crystal	crystal	NOUN
eurjchem-1922	28	9	were	be	AUX
eurjchem-1922	28	10	recorded	record	VERB
eurjchem-1922	28	11	using	use	VERB
eurjchem-1922	28	12	a	a	DET
eurjchem-1922	28	13	bruker	bruker	ADJ
eurjchem-1922	28	14	apex	apex	PROPN
eurjchem-1922	28	15	-	-	PUNCT
eurjchem-1922	28	16	ii	ii	PROPN
eurjchem-1922	28	17	ccd	ccd	PROPN
eurjchem-1922	28	18	diffractometer	diffractometer	NOUN
eurjchem-1922	29	1	[	[	X
eurjchem-1922	29	2	11	11	NUM
eurjchem-1922	29	3	]	]	PUNCT
eurjchem-1922	29	4	.	.	PUNCT
eurjchem-1922	30	1	the	the	DET
eurjchem-1922	30	2	electro	electro	NOUN
eurjchem-1922	30	3	spray	spray	VERB
eurjchem-1922	30	4	mass	mass	PROPN
eurjchem-1922	30	5	spectra	spectra	PROPN
eurjchem-1922	30	6	were	be	AUX
eurjchem-1922	30	7	recorded	record	VERB
eurjchem-1922	30	8	on	on	ADP
eurjchem-1922	30	9	a	a	DET
eurjchem-1922	30	10	thermo	thermo	NOUN
eurjchem-1922	30	11	finnigan	finnigan	NOUN
eurjchem-1922	30	12	lcq	lcq	PROPN
eurjchem-1922	30	13	advantage	advantage	NOUN
eurjchem-1922	30	14	max	max	PROPN
eurjchem-1922	30	15	ion	ion	NOUN
eurjchem-1922	30	16	trap	trap	NOUN
eurjchem-1922	30	17	mass	mass	NOUN
eurjchem-1922	30	18	spectrometer	spectrometer	NOUN
eurjchem-1922	30	19	.	.	PUNCT
eurjchem-1922	31	1	abstract	abstract	ADJ
eurjchem-1922	31	2	research	research	NOUN
eurjchem-1922	31	3	article	article	NOUN
eurjchem-1922	31	4	keywords	keyword	VERB
eurjchem-1922	31	5	european	european	PROPN
eurjchem-1922	31	6	journal	journal	PROPN
eurjchem-1922	31	7	of	of	ADP
eurjchem-1922	31	8	chemistry	chemistry	NOUN
eurjchem-1922	31	9	issn	issn	VERB
eurjchem-1922	31	10	2153	2153	NUM
eurjchem-1922	31	11	-	-	SYM
eurjchem-1922	31	12	2249	2249	NUM
eurjchem-1922	31	13	(	(	PUNCT
eurjchem-1922	31	14	print	print	NOUN
eurjchem-1922	31	15	)	)	PUNCT
eurjchem-1922	31	16	/	/	PUNCT
eurjchem-1922	31	17	issn	issn	PROPN
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eurjchem-1922	31	24	–	–	PUNCT
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eurjchem-1922	31	26	©	©	PROPN
eurjchem-1922	31	27	2019	2019	NUM
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eurjchem-1922	31	29	authors	author	NOUN
eurjchem-1922	31	30	–	–	PUNCT
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eurjchem-1922	31	33	house	house	PROPN
eurjchem-1922	31	34	llc	llc	PROPN
eurjchem-1922	31	35	–	–	PUNCT
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eurjchem-1922	31	39	usa	usa	PROPN
eurjchem-1922	31	40	.	.	PUNCT
eurjchem-1922	32	1	this	this	DET
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eurjchem-1922	32	8	atlanta	atlanta	PROPN
eurjchem-1922	32	9	publishing	publishing	PROPN
eurjchem-1922	32	10	house	house	PROPN
eurjchem-1922	32	11	llc	llc	PROPN
eurjchem-1922	32	12	–	–	PUNCT
eurjchem-1922	32	13	cc	cc	PROPN
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eurjchem-1922	32	16	–	–	PUNCT
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eurjchem-1922	33	9	mailto:jnvishwakarma@rediffmail.com	mailto:jnvishwakarma@rediffmail.com	PROPN
eurjchem-1922	33	10	mailto:jnvishwakarma@rediffmail.com	mailto:jnvishwakarma@rediffmail.com	PROPN
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eurjchem-1922	33	12	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.10.4.381-385.1922&domain=pdf&date_stamp=2019-12-31	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.10.4.381-385.1922&domain=pdf&date_stamp=2019-12-31	PROPN
eurjchem-1922	33	13	�	�	PROPN
eurjchem-1922	33	14	382	382	NUM
eurjchem-1922	33	15	nongrum	nongrum	NOUN
eurjchem-1922	33	16	et	et	PROPN
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eurjchem-1922	33	18	.	.	PUNCT
eurjchem-1922	33	19	/	/	SYM
eurjchem-1922	33	20	european	european	PROPN
eurjchem-1922	33	21	journal	journal	PROPN
eurjchem-1922	33	22	of	of	ADP
eurjchem-1922	33	23	chemistry	chemistry	NOUN
eurjchem-1922	33	24	10	10	NUM
eurjchem-1922	33	25	(	(	PUNCT
eurjchem-1922	33	26	4	4	NUM
eurjchem-1922	33	27	)	)	PUNCT
eurjchem-1922	33	28	(	(	PUNCT
eurjchem-1922	33	29	2019	2019	NUM
eurjchem-1922	33	30	)	)	PUNCT
eurjchem-1922	33	31	381	381	NUM
eurjchem-1922	33	32	-	-	SYM
eurjchem-1922	33	33	385	385	NUM
eurjchem-1922	33	34	cf3	cf3	NOUN
eurjchem-1922	33	35	f3c	f3c	NOUN
eurjchem-1922	33	36	n	n	PRON
eurjchem-1922	33	37	me	i	PRON
eurjchem-1922	33	38	me	i	PRON
eurjchem-1922	33	39	o	o	NOUN
eurjchem-1922	33	40	cf3	cf3	PROPN
eurjchem-1922	33	41	f3c	f3c	VERB
eurjchem-1922	33	42	me	i	PRON
eurjchem-1922	33	43	o	o	NOUN
eurjchem-1922	33	44	toluene	toluene	NOUN
eurjchem-1922	33	45	,	,	PUNCT
eurjchem-1922	33	46	reflux	reflux	VERB
eurjchem-1922	33	47	1	1	NUM
eurjchem-1922	33	48	3	3	NUM
eurjchem-1922	33	49	n	n	NOUN
eurjchem-1922	33	50	ch	ch	NOUN
eurjchem-1922	33	51	ome	ome	INTJ
eurjchem-1922	33	52	ome	ome	ADP
eurjchem-1922	33	53	me	i	PRON
eurjchem-1922	33	54	me	i	PRON
eurjchem-1922	33	55	20	20	NUM
eurjchem-1922	33	56	h	h	NOUN
eurjchem-1922	33	57	2	2	NUM
eurjchem-1922	33	58	scheme	scheme	NOUN
eurjchem-1922	33	59	1	1	NUM
eurjchem-1922	33	60	figure	figure	NOUN
eurjchem-1922	33	61	1	1	NUM
eurjchem-1922	33	62	.	.	PUNCT
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eurjchem-1922	33	67	title	title	NOUN
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eurjchem-1922	34	1	2.2	2.2	NUM
eurjchem-1922	34	2	.	.	PUNCT
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eurjchem-1922	34	4	a	a	DET
eurjchem-1922	34	5	mixture	mixture	NOUN
eurjchem-1922	34	6	of	of	ADP
eurjchem-1922	34	7	3,5	3,5	NUM
eurjchem-1922	34	8	-	-	PUNCT
eurjchem-1922	34	9	bis-(trifluoromethyl)acetophenone	bis-(trifluoromethyl)acetophenone	NOUN
eurjchem-1922	34	10	(	(	PUNCT
eurjchem-1922	34	11	1	1	NUM
eurjchem-1922	34	12	)	)	PUNCT
eurjchem-1922	34	13	(	(	PUNCT
eurjchem-1922	34	14	1	1	NUM
eurjchem-1922	34	15	mmol	mmol	NOUN
eurjchem-1922	34	16	)	)	PUNCT
eurjchem-1922	34	17	and	and	CCONJ
eurjchem-1922	34	18	n	n	CCONJ
eurjchem-1922	34	19	,	,	PUNCT
eurjchem-1922	34	20	n	n	CCONJ
eurjchem-1922	34	21	-	-	PUNCT
eurjchem-1922	34	22	dimethylformamide	dimethylformamide	NOUN
eurjchem-1922	34	23	dimethyl	dimethyl	NOUN
eurjchem-1922	34	24	acetal	acetal	NOUN
eurjchem-1922	34	25	(	(	PUNCT
eurjchem-1922	34	26	2	2	NUM
eurjchem-1922	34	27	)	)	PUNCT
eurjchem-1922	34	28	(	(	PUNCT
eurjchem-1922	34	29	2	2	NUM
eurjchem-1922	34	30	mmol	mmol	NOUN
eurjchem-1922	34	31	)	)	PUNCT
eurjchem-1922	34	32	in	in	ADP
eurjchem-1922	34	33	3	3	NUM
eurjchem-1922	34	34	ml	ml	NOUN
eurjchem-1922	34	35	toluene	toluene	NOUN
eurjchem-1922	34	36	was	be	AUX
eurjchem-1922	34	37	refluxed	refluxe	VERB
eurjchem-1922	34	38	for	for	ADP
eurjchem-1922	34	39	20	20	NUM
eurjchem-1922	34	40	hours	hour	NOUN
eurjchem-1922	34	41	.	.	PUNCT
eurjchem-1922	35	1	completion	completion	NOUN
eurjchem-1922	35	2	of	of	ADP
eurjchem-1922	35	3	the	the	DET
eurjchem-1922	35	4	reaction	reaction	NOUN
eurjchem-1922	35	5	was	be	AUX
eurjchem-1922	35	6	monitored	monitor	VERB
eurjchem-1922	35	7	by	by	ADP
eurjchem-1922	35	8	tlc	tlc	PROPN
eurjchem-1922	35	9	.	.	PUNCT
eurjchem-1922	36	1	at	at	ADP
eurjchem-1922	36	2	the	the	DET
eurjchem-1922	36	3	end	end	NOUN
eurjchem-1922	36	4	of	of	ADP
eurjchem-1922	36	5	the	the	DET
eurjchem-1922	36	6	reaction	reaction	NOUN
eurjchem-1922	36	7	,	,	PUNCT
eurjchem-1922	36	8	solvent	solvent	NOUN
eurjchem-1922	36	9	was	be	AUX
eurjchem-1922	36	10	removed	remove	VERB
eurjchem-1922	36	11	under	under	ADP
eurjchem-1922	36	12	reduced	reduce	VERB
eurjchem-1922	36	13	pressure	pressure	NOUN
eurjchem-1922	36	14	to	to	PART
eurjchem-1922	36	15	give	give	VERB
eurjchem-1922	36	16	a	a	DET
eurjchem-1922	36	17	viscous	viscous	ADJ
eurjchem-1922	36	18	mass	mass	NOUN
eurjchem-1922	36	19	which	which	PRON
eurjchem-1922	36	20	on	on	ADP
eurjchem-1922	36	21	trituration	trituration	NOUN
eurjchem-1922	36	22	with	with	ADP
eurjchem-1922	36	23	hexane	hexane	NOUN
eurjchem-1922	36	24	gave	give	VERB
eurjchem-1922	36	25	a	a	DET
eurjchem-1922	36	26	practically	practically	ADV
eurjchem-1922	36	27	pure	pure	ADJ
eurjchem-1922	36	28	yellow	yellow	ADJ
eurjchem-1922	36	29	solid	solid	ADJ
eurjchem-1922	36	30	in	in	ADP
eurjchem-1922	36	31	87	87	NUM
eurjchem-1922	36	32	%	%	NOUN
eurjchem-1922	36	33	yield	yield	NOUN
eurjchem-1922	36	34	.	.	PUNCT
eurjchem-1922	37	1	further	further	ADJ
eurjchem-1922	37	2	purification	purification	NOUN
eurjchem-1922	37	3	was	be	AUX
eurjchem-1922	37	4	achieved	achieve	VERB
eurjchem-1922	37	5	by	by	ADP
eurjchem-1922	37	6	column	column	NOUN
eurjchem-1922	37	7	chromatography	chromatography	NOUN
eurjchem-1922	37	8	on	on	ADP
eurjchem-1922	37	9	silica	silica	NOUN
eurjchem-1922	37	10	gel	gel	NOUN
eurjchem-1922	37	11	(	(	PUNCT
eurjchem-1922	37	12	60	60	NUM
eurjchem-1922	37	13	-	-	SYM
eurjchem-1922	37	14	120	120	NUM
eurjchem-1922	37	15	mesh	mesh	NOUN
eurjchem-1922	37	16	)	)	PUNCT
eurjchem-1922	37	17	using	use	VERB
eurjchem-1922	37	18	ethylacetate	ethylacetate	ADJ
eurjchem-1922	37	19	-	-	PUNCT
eurjchem-1922	37	20	hexane	hexane	NOUN
eurjchem-1922	37	21	(	(	PUNCT
eurjchem-1922	37	22	20	20	NUM
eurjchem-1922	37	23	%	%	NOUN
eurjchem-1922	37	24	)	)	PUNCT
eurjchem-1922	37	25	mixture	mixture	NOUN
eurjchem-1922	37	26	as	as	ADP
eurjchem-1922	37	27	mobile	mobile	ADJ
eurjchem-1922	37	28	phase	phase	NOUN
eurjchem-1922	37	29	.	.	PUNCT
eurjchem-1922	38	1	1-(3	1-(3	NUM
eurjchem-1922	38	2	,	,	PUNCT
eurjchem-1922	38	3	5	5	NUM
eurjchem-1922	38	4	-	-	PUNCT
eurjchem-1922	38	5	bis(trifluoromethyl)phenyl)-3-(dimethylamino)prop2	bis(trifluoromethyl)phenyl)-3-(dimethylamino)prop2	NUM
eurjchem-1922	38	6	-	-	PUNCT
eurjchem-1922	38	7	en-1	en-1	ADV
eurjchem-1922	38	8	-	-	PUNCT
eurjchem-1922	38	9	one	one	NUM
eurjchem-1922	38	10	(	(	PUNCT
eurjchem-1922	38	11	3	3	NUM
eurjchem-1922	38	12	):	):	PUNCT
eurjchem-1922	38	13	colour	colour	NOUN
eurjchem-1922	38	14	:	:	PUNCT
eurjchem-1922	38	15	yellow	yellow	ADJ
eurjchem-1922	38	16	.	.	PUNCT
eurjchem-1922	39	1	yield	yield	NOUN
eurjchem-1922	39	2	:	:	PUNCT
eurjchem-1922	39	3	87	87	NUM
eurjchem-1922	39	4	%	%	NOUN
eurjchem-1922	39	5	.	.	PUNCT
eurjchem-1922	40	1	m.p	m.p	PROPN
eurjchem-1922	40	2	.	.	PROPN
eurjchem-1922	40	3	:	:	PUNCT
eurjchem-1922	41	1	95	95	NUM
eurjchem-1922	41	2	-	-	SYM
eurjchem-1922	41	3	96	96	NUM
eurjchem-1922	41	4	°	°	NUM
eurjchem-1922	41	5	c	c	X
eurjchem-1922	41	6	.	.	PUNCT
eurjchem-1922	41	7	ftir	ftir	PROPN
eurjchem-1922	41	8	(	(	PUNCT
eurjchem-1922	41	9	kbr	kbr	PROPN
eurjchem-1922	41	10	,	,	PUNCT
eurjchem-1922	41	11	ν	ν	PROPN
eurjchem-1922	41	12	,	,	PUNCT
eurjchem-1922	41	13	cm-1	cm-1	NUM
eurjchem-1922	41	14	):	):	PUNCT
eurjchem-1922	41	15	1676	1676	NUM
eurjchem-1922	41	16	(	(	PUNCT
eurjchem-1922	41	17	c	c	NOUN
eurjchem-1922	41	18	=	=	NOUN
eurjchem-1922	41	19	o	o	NOUN
eurjchem-1922	41	20	)	)	PUNCT
eurjchem-1922	41	21	(	(	PUNCT
eurjchem-1922	41	22	ketone	ketone	NOUN
eurjchem-1922	41	23	)	)	PUNCT
eurjchem-1922	41	24	,	,	PUNCT
eurjchem-1922	41	25	1558	1558	NUM
eurjchem-1922	41	26	(	(	PUNCT
eurjchem-1922	41	27	c	c	NOUN
eurjchem-1922	41	28	=	=	SYM
eurjchem-1922	41	29	c	c	NOUN
eurjchem-1922	41	30	)	)	PUNCT
eurjchem-1922	41	31	(	(	PUNCT
eurjchem-1922	41	32	aromatic	aromatic	NOUN
eurjchem-1922	41	33	)	)	PUNCT
eurjchem-1922	41	34	,	,	PUNCT
eurjchem-1922	41	35	1348	1348	NUM
eurjchem-1922	41	36	(	(	PUNCT
eurjchem-1922	41	37	c	c	NOUN
eurjchem-1922	41	38	-	-	PUNCT
eurjchem-1922	41	39	n	n	CCONJ
eurjchem-1922	41	40	)	)	PUNCT
eurjchem-1922	41	41	(	(	PUNCT
eurjchem-1922	41	42	amine	amine	NOUN
eurjchem-1922	41	43	)	)	PUNCT
eurjchem-1922	41	44	,	,	PUNCT
eurjchem-1922	41	45	1295	1295	NUM
eurjchem-1922	41	46	(	(	PUNCT
eurjchem-1922	41	47	c	c	NOUN
eurjchem-1922	41	48	-	-	SYM
eurjchem-1922	41	49	f	f	NOUN
eurjchem-1922	41	50	)	)	PUNCT
eurjchem-1922	41	51	,	,	PUNCT
eurjchem-1922	41	52	910	910	NUM
eurjchem-1922	41	53	(	(	PUNCT
eurjchem-1922	41	54	c	c	NOUN
eurjchem-1922	41	55	-	-	PUNCT
eurjchem-1922	41	56	h	h	NOUN
eurjchem-1922	41	57	)	)	PUNCT
eurjchem-1922	41	58	(	(	PUNCT
eurjchem-1922	41	59	aromatic	aromatic	NOUN
eurjchem-1922	41	60	)	)	PUNCT
eurjchem-1922	41	61	,	,	PUNCT
eurjchem-1922	41	62	662	662	NUM
eurjchem-1922	41	63	(	(	PUNCT
eurjchem-1922	41	64	ch	ch	NOUN
eurjchem-1922	41	65	)	)	PUNCT
eurjchem-1922	41	66	(	(	PUNCT
eurjchem-1922	41	67	aromatic	aromatic	NOUN
eurjchem-1922	41	68	)	)	PUNCT
eurjchem-1922	41	69	.	.	PUNCT
eurjchem-1922	42	1	1h	1h	NUM
eurjchem-1922	42	2	nmr	nmr	NOUN
eurjchem-1922	42	3	(	(	PUNCT
eurjchem-1922	42	4	300	300	NUM
eurjchem-1922	42	5	mhz	mhz	NOUN
eurjchem-1922	42	6	,	,	PUNCT
eurjchem-1922	42	7	cdcl3	cdcl3	PROPN
eurjchem-1922	42	8	,	,	PUNCT
eurjchem-1922	42	9	δ	δ	PROPN
eurjchem-1922	42	10	,	,	PUNCT
eurjchem-1922	42	11	ppm	ppm	NUM
eurjchem-1922	42	12	):	):	PUNCT
eurjchem-1922	42	13	2.99	2.99	NUM
eurjchem-1922	42	14	(	(	PUNCT
eurjchem-1922	42	15	s	s	PROPN
eurjchem-1922	42	16	,	,	PUNCT
eurjchem-1922	42	17	3h	3h	NUM
eurjchem-1922	42	18	,	,	PUNCT
eurjchem-1922	42	19	ch3	ch3	PROPN
eurjchem-1922	42	20	)	)	PUNCT
eurjchem-1922	42	21	,	,	PUNCT
eurjchem-1922	42	22	3.22	3.22	NUM
eurjchem-1922	42	23	(	(	PUNCT
eurjchem-1922	42	24	s	s	PROPN
eurjchem-1922	42	25	,	,	PUNCT
eurjchem-1922	42	26	3h	3h	NUM
eurjchem-1922	42	27	,	,	PUNCT
eurjchem-1922	42	28	ch3	ch3	PROPN
eurjchem-1922	42	29	)	)	PUNCT
eurjchem-1922	42	30	,	,	PUNCT
eurjchem-1922	42	31	5.67	5.67	NUM
eurjchem-1922	42	32	(	(	PUNCT
eurjchem-1922	42	33	d	d	PROPN
eurjchem-1922	42	34	,	,	PUNCT
eurjchem-1922	42	35	1h	1h	NUM
eurjchem-1922	42	36	,	,	PUNCT
eurjchem-1922	42	37	j	j	PROPN
eurjchem-1922	42	38	=	=	PROPN
eurjchem-1922	42	39	12	12	NUM
eurjchem-1922	42	40	hz	hz	VERB
eurjchem-1922	42	41	,	,	PUNCT
eurjchem-1922	42	42	c2h	c2h	PROPN
eurjchem-1922	42	43	)	)	PUNCT
eurjchem-1922	42	44	,	,	PUNCT
eurjchem-1922	42	45	7.91	7.91	NUM
eurjchem-1922	42	46	(	(	PUNCT
eurjchem-1922	42	47	d	d	PROPN
eurjchem-1922	42	48	,	,	PUNCT
eurjchem-1922	42	49	1h	1h	NUM
eurjchem-1922	42	50	,	,	PUNCT
eurjchem-1922	42	51	j	j	PROPN
eurjchem-1922	42	52	=	=	PROPN
eurjchem-1922	42	53	12	12	NUM
eurjchem-1922	42	54	hz	hz	VERB
eurjchem-1922	42	55	,	,	PUNCT
eurjchem-1922	42	56	c3h	c3h	PROPN
eurjchem-1922	42	57	)	)	PUNCT
eurjchem-1922	42	58	,	,	PUNCT
eurjchem-1922	42	59	7.94	7.94	NUM
eurjchem-1922	42	60	(	(	PUNCT
eurjchem-1922	42	61	s	s	PROPN
eurjchem-1922	42	62	,	,	PUNCT
eurjchem-1922	42	63	1h	1h	NUM
eurjchem-1922	42	64	,	,	PUNCT
eurjchem-1922	42	65	ar	ar	NOUN
eurjchem-1922	42	66	-	-	NOUN
eurjchem-1922	42	67	h	h	NOUN
eurjchem-1922	42	68	)	)	PUNCT
eurjchem-1922	42	69	,	,	PUNCT
eurjchem-1922	42	70	8.32	8.32	NUM
eurjchem-1922	42	71	(	(	PUNCT
eurjchem-1922	42	72	s	s	PROPN
eurjchem-1922	42	73	,	,	PUNCT
eurjchem-1922	42	74	2h	2h	NUM
eurjchem-1922	42	75	,	,	PUNCT
eurjchem-1922	42	76	ar	ar	NOUN
eurjchem-1922	42	77	-	-	NOUN
eurjchem-1922	42	78	h	h	NOUN
eurjchem-1922	42	79	)	)	PUNCT
eurjchem-1922	42	80	.	.	PUNCT
eurjchem-1922	43	1	13c	13c	NOUN
eurjchem-1922	43	2	nmr	nmr	NOUN
eurjchem-1922	43	3	(	(	PUNCT
eurjchem-1922	43	4	75	75	NUM
eurjchem-1922	43	5	mhz	mhz	NOUN
eurjchem-1922	43	6	,	,	PUNCT
eurjchem-1922	43	7	cdcl3	cdcl3	PROPN
eurjchem-1922	43	8	,	,	PUNCT
eurjchem-1922	43	9	δ	δ	PROPN
eurjchem-1922	43	10	,	,	PUNCT
eurjchem-1922	43	11	ppm	ppm	NUM
eurjchem-1922	43	12	):	):	PUNCT
eurjchem-1922	43	13	37.7	37.7	NUM
eurjchem-1922	43	14	(	(	PUNCT
eurjchem-1922	43	15	1c	1c	NOUN
eurjchem-1922	43	16	,	,	PUNCT
eurjchem-1922	43	17	ch3	ch3	PROPN
eurjchem-1922	43	18	)	)	PUNCT
eurjchem-1922	43	19	,	,	PUNCT
eurjchem-1922	43	20	45.5	45.5	NUM
eurjchem-1922	43	21	(	(	PUNCT
eurjchem-1922	43	22	1c	1c	X
eurjchem-1922	43	23	,	,	PUNCT
eurjchem-1922	43	24	ch3	ch3	PROPN
eurjchem-1922	43	25	)	)	PUNCT
eurjchem-1922	43	26	,	,	PUNCT
eurjchem-1922	43	27	91.1	91.1	NUM
eurjchem-1922	43	28	(	(	PUNCT
eurjchem-1922	43	29	1c	1c	NOUN
eurjchem-1922	43	30	,	,	PUNCT
eurjchem-1922	43	31	c2	c2	PROPN
eurjchem-1922	43	32	)	)	PUNCT
eurjchem-1922	43	33	,	,	PUNCT
eurjchem-1922	43	34	123.5	123.5	NUM
eurjchem-1922	43	35	(	(	PUNCT
eurjchem-1922	43	36	2c	2c	NOUN
eurjchem-1922	43	37	,	,	PUNCT
eurjchem-1922	43	38	cf3	cf3	PROPN
eurjchem-1922	43	39	)	)	PUNCT
eurjchem-1922	43	40	,	,	PUNCT
eurjchem-1922	43	41	124.3	124.3	NUM
eurjchem-1922	43	42	(	(	PUNCT
eurjchem-1922	43	43	1c	1c	X
eurjchem-1922	43	44	,	,	PUNCT
eurjchem-1922	43	45	c4	c4	NOUN
eurjchem-1922	43	46	’	'	PUNCT
eurjchem-1922	43	47	,	,	PUNCT
eurjchem-1922	43	48	aromatic	aromatic	NOUN
eurjchem-1922	43	49	)	)	PUNCT
eurjchem-1922	43	50	,	,	PUNCT
eurjchem-1922	43	51	127.7	127.7	NUM
eurjchem-1922	43	52	(	(	PUNCT
eurjchem-1922	43	53	2c	2c	NUM
eurjchem-1922	43	54	,	,	PUNCT
eurjchem-1922	43	55	c2	c2	PROPN
eurjchem-1922	43	56	’	'	PUNCT
eurjchem-1922	43	57	,	,	PUNCT
eurjchem-1922	43	58	c6	c6	PROPN
eurjchem-1922	43	59	’	'	PUNCT
eurjchem-1922	43	60	,	,	PUNCT
eurjchem-1922	43	61	aromatic	aromatic	NOUN
eurjchem-1922	43	62	)	)	PUNCT
eurjchem-1922	43	63	,	,	PUNCT
eurjchem-1922	43	64	131.7	131.7	NUM
eurjchem-1922	43	65	(	(	PUNCT
eurjchem-1922	43	66	2c	2c	NUM
eurjchem-1922	43	67	,	,	PUNCT
eurjchem-1922	43	68	c3	c3	PROPN
eurjchem-1922	43	69	’	'	PUNCT
eurjchem-1922	43	70	,	,	PUNCT
eurjchem-1922	43	71	c5	c5	PROPN
eurjchem-1922	43	72	’	'	PUNCT
eurjchem-1922	43	73	,	,	PUNCT
eurjchem-1922	43	74	aromatic	aromatic	NOUN
eurjchem-1922	43	75	)	)	PUNCT
eurjchem-1922	43	76	,	,	PUNCT
eurjchem-1922	43	77	142.5	142.5	NUM
eurjchem-1922	43	78	(	(	PUNCT
eurjchem-1922	43	79	1c	1c	X
eurjchem-1922	43	80	,	,	PUNCT
eurjchem-1922	43	81	c1	c1	PROPN
eurjchem-1922	43	82	’	'	PUNCT
eurjchem-1922	43	83	,	,	PUNCT
eurjchem-1922	43	84	aromatic	aromatic	NOUN
eurjchem-1922	43	85	)	)	PUNCT
eurjchem-1922	43	86	,	,	PUNCT
eurjchem-1922	43	87	155.7	155.7	NUM
eurjchem-1922	43	88	(	(	PUNCT
eurjchem-1922	43	89	1c	1c	X
eurjchem-1922	43	90	,	,	PUNCT
eurjchem-1922	43	91	c3	c3	PROPN
eurjchem-1922	43	92	)	)	PUNCT
eurjchem-1922	43	93	,	,	PUNCT
eurjchem-1922	43	94	184.7	184.7	NUM
eurjchem-1922	43	95	(	(	PUNCT
eurjchem-1922	43	96	1c	1c	X
eurjchem-1922	43	97	,	,	PUNCT
eurjchem-1922	43	98	c1	c1	PROPN
eurjchem-1922	43	99	)	)	PUNCT
eurjchem-1922	43	100	.	.	PUNCT
eurjchem-1922	44	1	ms	ms	PROPN
eurjchem-1922	44	2	(	(	PUNCT
eurjchem-1922	44	3	esi	esi	PROPN
eurjchem-1922	44	4	,	,	PUNCT
eurjchem-1922	44	5	m	m	PROPN
eurjchem-1922	44	6	/	/	SYM
eurjchem-1922	44	7	z	z	PROPN
eurjchem-1922	44	8	(	(	PUNCT
eurjchem-1922	44	9	%	%	NOUN
eurjchem-1922	44	10	)	)	PUNCT
eurjchem-1922	44	11	):	):	PUNCT
eurjchem-1922	44	12	312	312	NUM
eurjchem-1922	44	13	(	(	PUNCT
eurjchem-1922	44	14	[	[	X
eurjchem-1922	44	15	mh]+	mh]+	X
eurjchem-1922	44	16	,	,	PUNCT
eurjchem-1922	44	17	100	100	NUM
eurjchem-1922	44	18	%	%	NOUN
eurjchem-1922	44	19	)	)	PUNCT
eurjchem-1922	44	20	,	,	PUNCT
eurjchem-1922	44	21	313	313	NUM
eurjchem-1922	44	22	,	,	PUNCT
eurjchem-1922	44	23	314	314	NUM
eurjchem-1922	44	24	,	,	PUNCT
eurjchem-1922	44	25	334	334	NUM
eurjchem-1922	44	26	,	,	PUNCT
eurjchem-1922	44	27	335	335	NUM
eurjchem-1922	44	28	.	.	PUNCT
eurjchem-1922	44	29	2.3	2.3	NUM
eurjchem-1922	44	30	.	.	PUNCT
eurjchem-1922	44	31	crystallographic	crystallographic	ADJ
eurjchem-1922	44	32	details	detail	NOUN
eurjchem-1922	44	33	block	block	NOUN
eurjchem-1922	44	34	,	,	PUNCT
eurjchem-1922	44	35	colorless	colorless	ADJ
eurjchem-1922	44	36	crystals	crystal	NOUN
eurjchem-1922	44	37	of	of	ADP
eurjchem-1922	44	38	the	the	DET
eurjchem-1922	44	39	compound	compound	NOUN
eurjchem-1922	44	40	were	be	AUX
eurjchem-1922	44	41	obtained	obtain	VERB
eurjchem-1922	44	42	by	by	ADP
eurjchem-1922	44	43	dissolving	dissolve	VERB
eurjchem-1922	44	44	the	the	DET
eurjchem-1922	44	45	compound	compound	NOUN
eurjchem-1922	44	46	in	in	ADP
eurjchem-1922	44	47	ethanol	ethanol	NOUN
eurjchem-1922	44	48	and	and	CCONJ
eurjchem-1922	44	49	then	then	ADV
eurjchem-1922	44	50	allowing	allow	VERB
eurjchem-1922	44	51	it	it	PRON
eurjchem-1922	44	52	to	to	PART
eurjchem-1922	44	53	recrystallize	recrystallize	VERB
eurjchem-1922	44	54	slowly	slowly	ADV
eurjchem-1922	44	55	.	.	PUNCT
eurjchem-1922	45	1	the	the	DET
eurjchem-1922	45	2	structure	structure	NOUN
eurjchem-1922	45	3	was	be	AUX
eurjchem-1922	45	4	solved	solve	VERB
eurjchem-1922	45	5	by	by	ADP
eurjchem-1922	45	6	direct	direct	ADJ
eurjchem-1922	45	7	methods	method	NOUN
eurjchem-1922	45	8	(	(	PUNCT
eurjchem-1922	45	9	shelxs97	shelxs97	PROPN
eurjchem-1922	45	10	)	)	PUNCT
eurjchem-1922	46	1	[	[	X
eurjchem-1922	46	2	12	12	NUM
eurjchem-1922	46	3	]	]	PUNCT
eurjchem-1922	46	4	and	and	CCONJ
eurjchem-1922	46	5	refined	refine	VERB
eurjchem-1922	46	6	by	by	ADP
eurjchem-1922	46	7	full	full	ADJ
eurjchem-1922	46	8	-	-	PUNCT
eurjchem-1922	46	9	matrix	matrix	NOUN
eurjchem-1922	46	10	leastsquares	leastsquare	NOUN
eurjchem-1922	46	11	based	base	VERB
eurjchem-1922	46	12	on	on	ADP
eurjchem-1922	46	13	f2	f2	PROPN
eurjchem-1922	46	14	.	.	PUNCT
eurjchem-1922	47	1	all	all	DET
eurjchem-1922	47	2	calculations	calculation	NOUN
eurjchem-1922	47	3	were	be	AUX
eurjchem-1922	47	4	carried	carry	VERB
eurjchem-1922	47	5	out	out	ADP
eurjchem-1922	47	6	using	use	VERB
eurjchem-1922	47	7	the	the	DET
eurjchem-1922	47	8	wingx	wingx	NOUN
eurjchem-1922	47	9	[	[	X
eurjchem-1922	47	10	13	13	NUM
eurjchem-1922	47	11	]	]	PUNCT
eurjchem-1922	47	12	system	system	NOUN
eurjchem-1922	47	13	version	version	NOUN
eurjchem-1922	47	14	1.80.05	1.80.05	PROPN
eurjchem-1922	47	15	.	.	PUNCT
eurjchem-1922	48	1	all	all	DET
eurjchem-1922	48	2	the	the	DET
eurjchem-1922	48	3	non	non	ADJ
eurjchem-1922	48	4	-	-	ADJ
eurjchem-1922	48	5	h	h	NOUN
eurjchem-1922	48	6	-	-	PUNCT
eurjchem-1922	48	7	atoms	atom	NOUN
eurjchem-1922	48	8	were	be	AUX
eurjchem-1922	48	9	refined	refine	VERB
eurjchem-1922	48	10	in	in	ADP
eurjchem-1922	48	11	the	the	DET
eurjchem-1922	48	12	anisotropic	anisotropic	NOUN
eurjchem-1922	48	13	approximation	approximation	NOUN
eurjchem-1922	48	14	.	.	PUNCT
eurjchem-1922	49	1	the	the	DET
eurjchem-1922	49	2	threshold	threshold	NOUN
eurjchem-1922	49	3	expression	expression	NOUN
eurjchem-1922	49	4	of	of	ADP
eurjchem-1922	49	5	f2>2sigma(f2	f2>2sigma(f2	PROPN
eurjchem-1922	49	6	)	)	PUNCT
eurjchem-1922	49	7	is	be	AUX
eurjchem-1922	49	8	used	use	VERB
eurjchem-1922	49	9	only	only	ADV
eurjchem-1922	49	10	for	for	ADP
eurjchem-1922	49	11	calculating	calculate	VERB
eurjchem-1922	49	12	rfactors	rfactor	NOUN
eurjchem-1922	49	13	(	(	PUNCT
eurjchem-1922	49	14	gt	gt	PROPN
eurjchem-1922	49	15	)	)	PUNCT
eurjchem-1922	49	16	etc	etc	X
eurjchem-1922	49	17	.	.	X
eurjchem-1922	50	1	h	h	NOUN
eurjchem-1922	50	2	-	-	PUNCT
eurjchem-1922	50	3	atoms	atom	NOUN
eurjchem-1922	50	4	were	be	AUX
eurjchem-1922	50	5	located	locate	VERB
eurjchem-1922	50	6	at	at	ADP
eurjchem-1922	50	7	calculated	calculate	VERB
eurjchem-1922	50	8	positions	position	NOUN
eurjchem-1922	50	9	.	.	PUNCT
eurjchem-1922	51	1	figure	figure	NOUN
eurjchem-1922	51	2	2	2	NUM
eurjchem-1922	51	3	shows	show	VERB
eurjchem-1922	51	4	the	the	DET
eurjchem-1922	51	5	packing	packing	NOUN
eurjchem-1922	51	6	pattern	pattern	NOUN
eurjchem-1922	51	7	of	of	ADP
eurjchem-1922	51	8	the	the	DET
eurjchem-1922	51	9	crystal	crystal	NOUN
eurjchem-1922	51	10	,	,	PUNCT
eurjchem-1922	51	11	of	of	ADP
eurjchem-1922	51	12	its	its	PRON
eurjchem-1922	51	13	components	component	NOUN
eurjchem-1922	51	14	in	in	ADP
eurjchem-1922	51	15	three	three	NUM
eurjchem-1922	51	16	dimensional	dimensional	ADJ
eurjchem-1922	51	17	lattice	lattice	NOUN
eurjchem-1922	51	18	.	.	PUNCT
eurjchem-1922	52	1	3	3	X
eurjchem-1922	52	2	.	.	X
eurjchem-1922	52	3	results	result	NOUN
eurjchem-1922	52	4	and	and	CCONJ
eurjchem-1922	52	5	discussion	discussion	NOUN
eurjchem-1922	52	6	3.1	3.1	NUM
eurjchem-1922	52	7	.	.	PUNCT
eurjchem-1922	53	1	spectral	spectral	ADJ
eurjchem-1922	53	2	analysis	analysis	NOUN
eurjchem-1922	53	3	the	the	DET
eurjchem-1922	53	4	ft	ft	PROPN
eurjchem-1922	53	5	-	-	PUNCT
eurjchem-1922	53	6	ir	ir	PROPN
eurjchem-1922	53	7	spectra	spectra	NOUN
eurjchem-1922	53	8	showed	show	VERB
eurjchem-1922	53	9	a	a	DET
eurjchem-1922	53	10	bands	band	NOUN
eurjchem-1922	53	11	at	at	ADP
eurjchem-1922	53	12	1676	1676	NUM
eurjchem-1922	53	13	cm-1	cm-1	VERB
eurjchem-1922	53	14	for	for	ADP
eurjchem-1922	53	15	c	c	NOUN
eurjchem-1922	53	16	=	=	NOUN
eurjchem-1922	53	17	o	o	NOUN
eurjchem-1922	53	18	,	,	PUNCT
eurjchem-1922	53	19	1558	1558	NUM
eurjchem-1922	53	20	cm-1	cm-1	VERB
eurjchem-1922	53	21	for	for	ADP
eurjchem-1922	53	22	c	c	NOUN
eurjchem-1922	53	23	=	=	SYM
eurjchem-1922	53	24	c	c	PROPN
eurjchem-1922	53	25	,	,	PUNCT
eurjchem-1922	53	26	1348	1348	NUM
eurjchem-1922	53	27	cm-1	cm-1	VERB
eurjchem-1922	53	28	for	for	ADP
eurjchem-1922	53	29	c	c	NOUN
eurjchem-1922	53	30	-	-	PUNCT
eurjchem-1922	53	31	n	n	CCONJ
eurjchem-1922	53	32	,	,	PUNCT
eurjchem-1922	53	33	1295	1295	NUM
eurjchem-1922	53	34	cm-1	cm-1	VERB
eurjchem-1922	53	35	for	for	ADP
eurjchem-1922	53	36	c	c	PROPN
eurjchem-1922	53	37	-	-	PUNCT
eurjchem-1922	53	38	f	f	PROPN
eurjchem-1922	53	39	and	and	CCONJ
eurjchem-1922	53	40	910	910	NUM
eurjchem-1922	53	41	cm-1	cm-1	NOUN
eurjchem-1922	53	42	and	and	CCONJ
eurjchem-1922	53	43	662	662	NUM
eurjchem-1922	53	44	cm-1	cm-1	NOUN
eurjchem-1922	53	45	for	for	ADP
eurjchem-1922	53	46	aromatic	aromatic	ADJ
eurjchem-1922	53	47	c	c	NOUN
eurjchem-1922	53	48	-	-	PUNCT
eurjchem-1922	53	49	h	h	NOUN
eurjchem-1922	53	50	bonds	bond	NOUN
eurjchem-1922	53	51	.	.	PUNCT
eurjchem-1922	54	1	the	the	DET
eurjchem-1922	54	2	1h	1h	NUM
eurjchem-1922	54	3	nmr	nmr	NOUN
eurjchem-1922	54	4	spectra	spectra	NOUN
eurjchem-1922	54	5	of	of	ADP
eurjchem-1922	54	6	compound	compound	NOUN
eurjchem-1922	54	7	3	3	NUM
eurjchem-1922	54	8	exhibited	exhibit	VERB
eurjchem-1922	54	9	two	two	NUM
eurjchem-1922	54	10	distinct	distinct	ADJ
eurjchem-1922	54	11	singlets	singlet	NOUN
eurjchem-1922	54	12	at	at	ADP
eurjchem-1922	54	13	δ	δ	PROPN
eurjchem-1922	54	14	2.99	2.99	NUM
eurjchem-1922	54	15	and	and	CCONJ
eurjchem-1922	54	16	3.22	3.22	NUM
eurjchem-1922	54	17	ppm	ppm	NOUN
eurjchem-1922	54	18	for	for	ADP
eurjchem-1922	54	19	the	the	DET
eurjchem-1922	54	20	two	two	NUM
eurjchem-1922	54	21	methyl	methyl	NOUN
eurjchem-1922	54	22	protons	proton	NOUN
eurjchem-1922	54	23	of	of	ADP
eurjchem-1922	54	24	nme2	nme2	PROPN
eurjchem-1922	54	25	group	group	NOUN
eurjchem-1922	54	26	indicating	indicate	VERB
eurjchem-1922	54	27	that	that	SCONJ
eurjchem-1922	54	28	the	the	DET
eurjchem-1922	54	29	two	two	NUM
eurjchem-1922	54	30	methyl	methyl	NOUN
eurjchem-1922	54	31	groups	group	NOUN
eurjchem-1922	54	32	are	be	AUX
eurjchem-1922	54	33	in	in	ADP
eurjchem-1922	54	34	different	different	ADJ
eurjchem-1922	54	35	environments	environment	NOUN
eurjchem-1922	54	36	due	due	ADJ
eurjchem-1922	54	37	the	the	DET
eurjchem-1922	54	38	double	double	ADJ
eurjchem-1922	54	39	bond	bond	NOUN
eurjchem-1922	54	40	character	character	NOUN
eurjchem-1922	54	41	of	of	ADP
eurjchem-1922	54	42	the	the	DET
eurjchem-1922	54	43	c	c	PROPN
eurjchem-1922	54	44	-	-	PUNCT
eurjchem-1922	54	45	n	n	PRON
eurjchem-1922	54	46	bond	bond	NOUN
eurjchem-1922	54	47	.	.	PUNCT
eurjchem-1922	55	1	the	the	DET
eurjchem-1922	55	2	vinylic	vinylic	ADJ
eurjchem-1922	55	3	protons	proton	NOUN
eurjchem-1922	55	4	resonated	resonate	VERB
eurjchem-1922	55	5	as	as	ADP
eurjchem-1922	55	6	doublets	doublet	NOUN
eurjchem-1922	55	7	at	at	ADP
eurjchem-1922	55	8	δ	δ	PROPN
eurjchem-1922	55	9	5.67	5.67	NUM
eurjchem-1922	55	10	and	and	CCONJ
eurjchem-1922	55	11	7.91	7.91	NUM
eurjchem-1922	55	12	ppm	ppm	NOUN
eurjchem-1922	55	13	with	with	ADP
eurjchem-1922	55	14	coupling	couple	VERB
eurjchem-1922	55	15	constant	constant	ADJ
eurjchem-1922	55	16	of	of	ADP
eurjchem-1922	55	17	12.0	12.0	NUM
eurjchem-1922	55	18	hz	hz	NOUN
eurjchem-1922	55	19	,	,	PUNCT
eurjchem-1922	55	20	thus	thus	ADV
eurjchem-1922	55	21	supporting	support	VERB
eurjchem-1922	55	22	trans	tran	NOUN
eurjchem-1922	55	23	geometry	geometry	NOUN
eurjchem-1922	55	24	.	.	PUNCT
eurjchem-1922	56	1	the	the	DET
eurjchem-1922	56	2	aromatic	aromatic	ADJ
eurjchem-1922	56	3	protons	proton	NOUN
eurjchem-1922	56	4	appeared	appear	VERB
eurjchem-1922	56	5	as	as	ADP
eurjchem-1922	56	6	singlets	singlet	NOUN
eurjchem-1922	56	7	at	at	ADP
eurjchem-1922	56	8	δ	δ	PROPN
eurjchem-1922	56	9	7.94	7.94	NUM
eurjchem-1922	56	10	ppm	ppm	NOUN
eurjchem-1922	56	11	for	for	ADP
eurjchem-1922	56	12	one	one	NUM
eurjchem-1922	56	13	proton	proton	NOUN
eurjchem-1922	56	14	and	and	CCONJ
eurjchem-1922	56	15	at	at	ADP
eurjchem-1922	56	16	δ	δ	PROPN
eurjchem-1922	56	17	8.32	8.32	NUM
eurjchem-1922	56	18	ppm	ppm	NOUN
eurjchem-1922	56	19	for	for	ADP
eurjchem-1922	56	20	two	two	NUM
eurjchem-1922	56	21	protons	proton	NOUN
eurjchem-1922	56	22	.	.	PUNCT
eurjchem-1922	57	1	in	in	ADP
eurjchem-1922	57	2	the	the	DET
eurjchem-1922	57	3	13c	13c	NOUN
eurjchem-1922	57	4	nmr	nmr	NOUN
eurjchem-1922	57	5	spectra	spectra	NOUN
eurjchem-1922	57	6	of	of	ADP
eurjchem-1922	57	7	compound	compound	NOUN
eurjchem-1922	57	8	3	3	NUM
eurjchem-1922	57	9	,	,	PUNCT
eurjchem-1922	57	10	the	the	DET
eurjchem-1922	57	11	two	two	NUM
eurjchem-1922	57	12	methyl	methyl	NOUN
eurjchem-1922	57	13	group	group	NOUN
eurjchem-1922	57	14	carbon	carbon	NOUN
eurjchem-1922	57	15	atoms	atom	NOUN
eurjchem-1922	57	16	showed	show	VERB
eurjchem-1922	57	17	signals	signal	NOUN
eurjchem-1922	57	18	at	at	ADP
eurjchem-1922	57	19	δ	δ	PROPN
eurjchem-1922	57	20	37.7	37.7	NUM
eurjchem-1922	57	21	and	and	CCONJ
eurjchem-1922	57	22	45.5	45.5	NUM
eurjchem-1922	57	23	ppm	ppm	NOUN
eurjchem-1922	57	24	.	.	PUNCT
eurjchem-1922	58	1	the	the	DET
eurjchem-1922	58	2	vinylic	vinylic	ADJ
eurjchem-1922	58	3	carbon	carbon	NOUN
eurjchem-1922	58	4	atoms	atom	NOUN
eurjchem-1922	58	5	c3	c3	PROPN
eurjchem-1922	58	6	and	and	CCONJ
eurjchem-1922	58	7	c2	c2	PROPN
eurjchem-1922	58	8	resonated	resonate	VERB
eurjchem-1922	58	9	at	at	ADP
eurjchem-1922	58	10	δ	δ	PROPN
eurjchem-1922	58	11	91.1	91.1	NUM
eurjchem-1922	58	12	and	and	CCONJ
eurjchem-1922	58	13	155.7	155.7	NUM
eurjchem-1922	58	14	ppm	ppm	NOUN
eurjchem-1922	58	15	,	,	PUNCT
eurjchem-1922	58	16	respectively	respectively	ADV
eurjchem-1922	58	17	.	.	PUNCT
eurjchem-1922	59	1	the	the	DET
eurjchem-1922	59	2	carbonyl	carbonyl	NOUN
eurjchem-1922	59	3	carbon	carbon	NOUN
eurjchem-1922	59	4	signal	signal	NOUN
eurjchem-1922	59	5	was	be	AUX
eurjchem-1922	59	6	found	find	VERB
eurjchem-1922	59	7	at	at	ADP
eurjchem-1922	59	8	δ	δ	PROPN
eurjchem-1922	59	9	184.7	184.7	NUM
eurjchem-1922	59	10	ppm	ppm	NOUN
eurjchem-1922	59	11	as	as	SCONJ
eurjchem-1922	59	12	expected	expect	VERB
eurjchem-1922	59	13	.	.	PUNCT
eurjchem-1922	60	1	the	the	DET
eurjchem-1922	60	2	13c	13c	NUM
eurjchem-1922	60	3	nmr	nmr	NOUN
eurjchem-1922	60	4	spectra	spectra	NOUN
eurjchem-1922	60	5	of	of	ADP
eurjchem-1922	60	6	the	the	DET
eurjchem-1922	60	7	aromatic	aromatic	ADJ
eurjchem-1922	60	8	ring	ring	NOUN
eurjchem-1922	60	9	was	be	AUX
eurjchem-1922	60	10	very	very	ADV
eurjchem-1922	60	11	interesting	interesting	ADJ
eurjchem-1922	60	12	due	due	ADP
eurjchem-1922	60	13	to	to	ADP
eurjchem-1922	60	14	coupling	couple	VERB
eurjchem-1922	60	15	pattern	pattern	NOUN
eurjchem-1922	60	16	with	with	ADP
eurjchem-1922	60	17	fluorine	fluorine	NOUN
eurjchem-1922	60	18	atoms	atom	NOUN
eurjchem-1922	60	19	.	.	PUNCT
eurjchem-1922	61	1	thus	thus	ADV
eurjchem-1922	61	2	,	,	PUNCT
eurjchem-1922	61	3	the	the	DET
eurjchem-1922	61	4	carbon	carbon	NOUN
eurjchem-1922	61	5	atoms	atom	NOUN
eurjchem-1922	61	6	of	of	ADP
eurjchem-1922	61	7	the	the	DET
eurjchem-1922	61	8	cf3	cf3	NOUN
eurjchem-1922	61	9	groups	group	NOUN
eurjchem-1922	61	10	gave	give	VERB
eurjchem-1922	61	11	quartet	quartet	NOUN
eurjchem-1922	61	12	at	at	ADP
eurjchem-1922	61	13	δ	δ	PROPN
eurjchem-1922	61	14	123.5	123.5	NUM
eurjchem-1922	61	15	ppm	ppm	NOUN
eurjchem-1922	61	16	with	with	ADP
eurjchem-1922	61	17	coupling	couple	VERB
eurjchem-1922	61	18	constant	constant	ADJ
eurjchem-1922	61	19	of	of	ADP
eurjchem-1922	61	20	270	270	NUM
eurjchem-1922	61	21	hz	hz	NOUN
eurjchem-1922	61	22	and	and	CCONJ
eurjchem-1922	61	23	the	the	DET
eurjchem-1922	61	24	aromatic	aromatic	ADJ
eurjchem-1922	61	25	carbon	carbon	NOUN
eurjchem-1922	61	26	atoms	atom	NOUN
eurjchem-1922	61	27	c3	c3	NOUN
eurjchem-1922	61	28	’	'	PUNCT
eurjchem-1922	61	29	and	and	CCONJ
eurjchem-1922	61	30	c5	c5	PROPN
eurjchem-1922	61	31	’	'	PUNCT
eurjchem-1922	61	32	appeared	appear	VERB
eurjchem-1922	61	33	as	as	ADP
eurjchem-1922	61	34	quartet	quartet	NOUN
eurjchem-1922	61	35	at	at	ADP
eurjchem-1922	61	36	δ	δ	PROPN
eurjchem-1922	61	37	131.7	131.7	NUM
eurjchem-1922	61	38	ppm	ppm	NOUN
eurjchem-1922	61	39	with	with	ADP
eurjchem-1922	61	40	a	a	DET
eurjchem-1922	61	41	coupling	coupling	NOUN
eurjchem-1922	61	42	constant	constant	ADJ
eurjchem-1922	61	43	of	of	ADP
eurjchem-1922	61	44	132	132	NUM
eurjchem-1922	61	45	hz	hz	NOUN
eurjchem-1922	61	46	.	.	PUNCT
eurjchem-1922	62	1	the	the	DET
eurjchem-1922	62	2	c4	c4	NOUN
eurjchem-1922	62	3	’	'	PUNCT
eurjchem-1922	62	4	of	of	ADP
eurjchem-1922	62	5	the	the	DET
eurjchem-1922	62	6	aromatic	aromatic	ADJ
eurjchem-1922	62	7	ring	ring	NOUN
eurjchem-1922	62	8	resonated	resonate	VERB
eurjchem-1922	62	9	at	at	ADP
eurjchem-1922	62	10	δ	δ	PROPN
eurjchem-1922	62	11	124.3	124.3	NUM
eurjchem-1922	62	12	ppm	ppm	NOUN
eurjchem-1922	62	13	as	as	ADP
eurjchem-1922	62	14	a	a	DET
eurjchem-1922	62	15	septet	septet	NOUN
eurjchem-1922	62	16	with	with	ADP
eurjchem-1922	62	17	a	a	DET
eurjchem-1922	62	18	coupling	coupling	NOUN
eurjchem-1922	62	19	constant	constant	ADJ
eurjchem-1922	62	20	3.75	3.75	NUM
eurjchem-1922	62	21	hz	hz	NOUN
eurjchem-1922	62	22	and	and	CCONJ
eurjchem-1922	62	23	c2	c2	PROPN
eurjchem-1922	62	24	’	'	PUNCT
eurjchem-1922	62	25	and	and	CCONJ
eurjchem-1922	62	26	c6	c6	PROPN
eurjchem-1922	62	27	’	'	PUNCT
eurjchem-1922	62	28	appeared	appear	VERB
eurjchem-1922	62	29	as	as	ADP
eurjchem-1922	62	30	a	a	DET
eurjchem-1922	62	31	doublet	doublet	NOUN
eurjchem-1922	62	32	at	at	ADP
eurjchem-1922	62	33	δ	δ	PROPN
eurjchem-1922	62	34	127.7	127.7	NUM
eurjchem-1922	62	35	ppm	ppm	NOUN
eurjchem-1922	62	36	with	with	ADP
eurjchem-1922	62	37	j	j	PROPN
eurjchem-1922	62	38	=	=	SYM
eurjchem-1922	62	39	3	3	NUM
eurjchem-1922	62	40	hz	hz	VERB
eurjchem-1922	62	41	.	.	PUNCT
eurjchem-1922	63	1	the	the	DET
eurjchem-1922	63	2	c1	c1	PROPN
eurjchem-1922	63	3	’	'	PUNCT
eurjchem-1922	63	4	carbon	carbon	NOUN
eurjchem-1922	63	5	was	be	AUX
eurjchem-1922	63	6	located	locate	VERB
eurjchem-1922	63	7	at	at	ADP
eurjchem-1922	63	8	δ	δ	PROPN
eurjchem-1922	63	9	142.5	142.5	NUM
eurjchem-1922	63	10	ppm	ppm	NOUN
eurjchem-1922	63	11	.	.	PUNCT
eurjchem-1922	64	1	the	the	DET
eurjchem-1922	64	2	mass	mass	ADJ
eurjchem-1922	64	3	spectra	spectra	NOUN
eurjchem-1922	64	4	of	of	ADP
eurjchem-1922	64	5	compound	compound	NOUN
eurjchem-1922	64	6	3	3	NUM
eurjchem-1922	64	7	showed	show	VERB
eurjchem-1922	64	8	a	a	DET
eurjchem-1922	64	9	base	base	NOUN
eurjchem-1922	64	10	peak	peak	NOUN
eurjchem-1922	64	11	for	for	ADP
eurjchem-1922	64	12	mh+	mh+	NOUN
eurjchem-1922	64	13	at	at	ADP
eurjchem-1922	64	14	312	312	NUM
eurjchem-1922	64	15	and	and	CCONJ
eurjchem-1922	64	16	other	other	ADJ
eurjchem-1922	64	17	peaks	peak	NOUN
eurjchem-1922	64	18	at	at	ADP
eurjchem-1922	64	19	313	313	NUM
eurjchem-1922	64	20	,	,	PUNCT
eurjchem-1922	64	21	314	314	NUM
eurjchem-1922	64	22	,	,	PUNCT
eurjchem-1922	64	23	334	334	NUM
eurjchem-1922	64	24	and	and	CCONJ
eurjchem-1922	64	25	335	335	NUM
eurjchem-1922	64	26	m	m	NOUN
eurjchem-1922	64	27	/	/	SYM
eurjchem-1922	64	28	z.	z.	PROPN
eurjchem-1922	64	29	dimethylformamide	dimethylformamide	NOUN
eurjchem-1922	64	30	-	-	PUNCT
eurjchem-1922	64	31	dimethylacetal	dimethylacetal	ADJ
eurjchem-1922	64	32	undergoes	undergoe	NOUN
eurjchem-1922	64	33	cleavage	cleavage	NOUN
eurjchem-1922	64	34	under	under	ADP
eurjchem-1922	64	35	thermal	thermal	ADJ
eurjchem-1922	64	36	conditions	condition	NOUN
eurjchem-1922	64	37	to	to	PART
eurjchem-1922	64	38	give	give	VERB
eurjchem-1922	64	39	the	the	DET
eurjchem-1922	64	40	oxo	oxo	NOUN
eurjchem-1922	64	41	-	-	PUNCT
eurjchem-1922	64	42	stabilized	stabilize	VERB
eurjchem-1922	64	43	carbenium	carbenium	NOUN
eurjchem-1922	64	44	ion	ion	NOUN
eurjchem-1922	64	45	a	a	NOUN
eurjchem-1922	64	46	,	,	PUNCT
eurjchem-1922	64	47	which	which	PRON
eurjchem-1922	64	48	acting	act	VERB
eurjchem-1922	64	49	as	as	ADP
eurjchem-1922	64	50	an	an	DET
eurjchem-1922	64	51	electrophile	electrophile	ADJ
eurjchem-1922	64	52	reacts	react	NOUN
eurjchem-1922	64	53	with	with	ADP
eurjchem-1922	64	54	enolized	enolize	VERB
eurjchem-1922	64	55	acetophenone	acetophenone	NOUN
eurjchem-1922	64	56	1	1	NUM
eurjchem-1922	64	57	to	to	PART
eurjchem-1922	64	58	give	give	VERB
eurjchem-1922	64	59	an	an	DET
eurjchem-1922	64	60	intermediate	intermediate	ADJ
eurjchem-1922	64	61	b.	b.	NOUN
eurjchem-1922	64	62	assisted	assist	VERB
eurjchem-1922	64	63	by	by	ADP
eurjchem-1922	64	64	the	the	DET
eurjchem-1922	64	65	methoxide	methoxide	PROPN
eurjchem-1922	64	66	ion	ion	NOUN
eurjchem-1922	64	67	b	b	PROPN
eurjchem-1922	64	68	is	be	AUX
eurjchem-1922	64	69	finally	finally	ADV
eurjchem-1922	64	70	converted	convert	VERB
eurjchem-1922	64	71	into	into	ADP
eurjchem-1922	64	72	the	the	DET
eurjchem-1922	64	73	desired	desire	VERB
eurjchem-1922	64	74	formaylated	formaylate	VERB
eurjchem-1922	64	75	acetophenone	acetophenone	NOUN
eurjchem-1922	64	76	3	3	NUM
eurjchem-1922	64	77	as	as	SCONJ
eurjchem-1922	64	78	shown	show	VERB
eurjchem-1922	64	79	in	in	ADP
eurjchem-1922	64	80	scheme	scheme	NOUN
eurjchem-1922	64	81	2	2	NUM
eurjchem-1922	64	82	.	.	SYM
eurjchem-1922	64	83	2019	2019	NUM
eurjchem-1922	64	84	–	–	PUNCT
eurjchem-1922	64	85	european	european	ADJ
eurjchem-1922	64	86	journal	journal	NOUN
eurjchem-1922	64	87	of	of	ADP
eurjchem-1922	64	88	chemistry	chemistry	NOUN
eurjchem-1922	64	89	–	–	PUNCT
eurjchem-1922	64	90	cc	cc	NOUN
eurjchem-1922	64	91	by	by	ADP
eurjchem-1922	64	92	nc	nc	PROPN
eurjchem-1922	64	93	–	–	PUNCT
eurjchem-1922	64	94	doi	doi	PROPN
eurjchem-1922	64	95	:	:	PUNCT
eurjchem-1922	64	96	10.5155	10.5155	NUM
eurjchem-1922	64	97	/	/	SYM
eurjchem-1922	64	98	eurjchem.10.4.381	eurjchem.10.4.381	NOUN
eurjchem-1922	64	99	-	-	PUNCT
eurjchem-1922	64	100	385.1922	385.1922	NUM
eurjchem-1922	64	101	nongrum	nongrum	NOUN
eurjchem-1922	64	102	et	et	PROPN
eurjchem-1922	64	103	al	al	PROPN
eurjchem-1922	64	104	.	.	PUNCT
eurjchem-1922	64	105	/	/	SYM
eurjchem-1922	64	106	european	european	PROPN
eurjchem-1922	64	107	journal	journal	PROPN
eurjchem-1922	64	108	of	of	ADP
eurjchem-1922	64	109	chemistry	chemistry	NOUN
eurjchem-1922	64	110	10	10	NUM
eurjchem-1922	64	111	(	(	PUNCT
eurjchem-1922	64	112	4	4	NUM
eurjchem-1922	64	113	)	)	PUNCT
eurjchem-1922	64	114	(	(	PUNCT
eurjchem-1922	64	115	2019	2019	NUM
eurjchem-1922	64	116	)	)	PUNCT
eurjchem-1922	64	117	381	381	NUM
eurjchem-1922	64	118	-	-	SYM
eurjchem-1922	64	119	385	385	NUM
eurjchem-1922	64	120	383	383	NUM
eurjchem-1922	64	121	f3c	f3c	NOUN
eurjchem-1922	65	1	cf3	cf3	PROPN
eurjchem-1922	65	2	c	c	PROPN
eurjchem-1922	65	3	h2	h2	PROPN
eurjchem-1922	65	4	o	o	INTJ
eurjchem-1922	65	5	cf3	cf3	PROPN
eurjchem-1922	65	6	f3ch	f3ch	VERB
eurjchem-1922	65	7	ch2	ch2	NOUN
eurjchem-1922	65	8	o	o	NOUN
eurjchem-1922	65	9	+	+	CCONJ
eurjchem-1922	65	10	h	h	NOUN
eurjchem-1922	65	11	f3c	f3c	NOUN
eurjchem-1922	65	12	cf3	cf3	NOUN
eurjchem-1922	65	13	o	o	NOUN
eurjchem-1922	65	14	h	h	NOUN
eurjchem-1922	65	15	ome	ome	PROPN
eurjchem-1922	65	16	nme2	nme2	PROPN
eurjchem-1922	65	17	f3c	f3c	VERB
eurjchem-1922	65	18	cf3	cf3	PROPN
eurjchem-1922	65	19	o	o	PROPN
eurjchem-1922	65	20	nme2	nme2	PROPN
eurjchem-1922	65	21	1	1	NUM
eurjchem-1922	65	22	3	3	NUM
eurjchem-1922	65	23	n	n	NOUN
eurjchem-1922	65	24	c	c	VERB
eurjchem-1922	65	25	me	i	PRON
eurjchem-1922	65	26	me	i	PRON
eurjchem-1922	65	27	ome	ome	INTJ
eurjchem-1922	65	28	ome	ome	PROPN
eurjchem-1922	65	29	h	h	NOUN
eurjchem-1922	65	30	heat	heat	NOUN
eurjchem-1922	66	1	n	n	ADP
eurjchem-1922	66	2	c	c	VERB
eurjchem-1922	66	3	me	i	PRON
eurjchem-1922	66	4	me	i	PRON
eurjchem-1922	67	1	ome	ome	PROPN
eurjchem-1922	67	2	h	h	NOUN
eurjchem-1922	68	1	n	n	ADV
eurjchem-1922	68	2	c	c	VERB
eurjchem-1922	68	3	me	i	PRON
eurjchem-1922	68	4	me	i	PRON
eurjchem-1922	69	1	ome	ome	NOUN
eurjchem-1922	69	2	h	h	NOUN
eurjchem-1922	69	3	2	2	NUM
eurjchem-1922	70	1	+	+	CCONJ
eurjchem-1922	70	2	a	a	DET
eurjchem-1922	70	3	a	a	DET
eurjchem-1922	70	4	b	b	NOUN
eurjchem-1922	70	5	ome	ome	NOUN
eurjchem-1922	70	6	ome	ome	NOUN
eurjchem-1922	70	7	scheme	scheme	NOUN
eurjchem-1922	70	8	2	2	NUM
eurjchem-1922	70	9	3.2	3.2	NUM
eurjchem-1922	70	10	.	.	PUNCT
eurjchem-1922	71	1	crystal	crystal	NOUN
eurjchem-1922	71	2	structure	structure	NOUN
eurjchem-1922	71	3	the	the	DET
eurjchem-1922	71	4	compound	compound	NOUN
eurjchem-1922	71	5	1-(3,5	1-(3,5	PROPN
eurjchem-1922	71	6	-	-	PUNCT
eurjchem-1922	71	7	bis(trifluoromethyl)phenyl)-3-(di	bis(trifluoromethyl)phenyl)-3-(di	ADJ
eurjchem-1922	71	8	methylamino)prop-2	methylamino)prop-2	NUM
eurjchem-1922	71	9	-	-	PUNCT
eurjchem-1922	71	10	en-1	en-1	NOUN
eurjchem-1922	71	11	-	-	PUNCT
eurjchem-1922	71	12	one	one	NUM
eurjchem-1922	71	13	(	(	PUNCT
eurjchem-1922	71	14	c13h11f6no	c13h11f6no	PROPN
eurjchem-1922	71	15	)	)	PUNCT
eurjchem-1922	71	16	crystallized	crystallize	VERB
eurjchem-1922	71	17	in	in	ADP
eurjchem-1922	71	18	a	a	DET
eurjchem-1922	71	19	monoclinic	monoclinic	ADJ
eurjchem-1922	71	20	cell	cell	NOUN
eurjchem-1922	71	21	(	(	PUNCT
eurjchem-1922	71	22	space	space	NOUN
eurjchem-1922	71	23	group	group	NOUN
eurjchem-1922	71	24	p2(1)/c	p2(1)/c	PROPN
eurjchem-1922	71	25	)	)	PUNCT
eurjchem-1922	71	26	obtained	obtain	VERB
eurjchem-1922	71	27	by	by	ADP
eurjchem-1922	71	28	phi	phi	NOUN
eurjchem-1922	71	29	and	and	CCONJ
eurjchem-1922	71	30	ῳ	ῳ	DET
eurjchem-1922	71	31	scans	scan	NOUN
eurjchem-1922	71	32	,	,	PUNCT
eurjchem-1922	71	33	refinement	refinement	NOUN
eurjchem-1922	71	34	on	on	ADP
eurjchem-1922	71	35	f2	f2	PROPN
eurjchem-1922	71	36	,	,	PUNCT
eurjchem-1922	71	37	r[f2>2σ(f2	r[f2>2σ(f2	PROPN
eurjchem-1922	71	38	)	)	PUNCT
eurjchem-1922	71	39	]	]	PUNCT
eurjchem-1922	72	1	=	=	SYM
eurjchem-1922	72	2	0.0771	0.0771	NUM
eurjchem-1922	72	3	,	,	PUNCT
eurjchem-1922	72	4	wr(f2	wr(f2	NOUN
eurjchem-1922	72	5	)	)	PUNCT
eurjchem-1922	72	6	=	=	SYM
eurjchem-1922	72	7	0.2541	0.2541	NUM
eurjchem-1922	72	8	,	,	PUNCT
eurjchem-1922	72	9	234	234	NUM
eurjchem-1922	72	10	parameters	parameter	NOUN
eurjchem-1922	72	11	and	and	CCONJ
eurjchem-1922	72	12	radiation	radiation	NOUN
eurjchem-1922	72	13	source	source	NOUN
eurjchem-1922	72	14	is	be	AUX
eurjchem-1922	72	15	from	from	ADP
eurjchem-1922	72	16	finefocus	finefocus	PROPN
eurjchem-1922	72	17	sealed	seal	VERB
eurjchem-1922	72	18	tube	tube	NOUN
eurjchem-1922	72	19	.	.	PUNCT
eurjchem-1922	73	1	all	all	DET
eurjchem-1922	73	2	the	the	DET
eurjchem-1922	73	3	conditions	condition	NOUN
eurjchem-1922	73	4	used	use	VERB
eurjchem-1922	73	5	for	for	ADP
eurjchem-1922	73	6	the	the	DET
eurjchem-1922	73	7	measurement	measurement	NOUN
eurjchem-1922	73	8	of	of	ADP
eurjchem-1922	73	9	the	the	DET
eurjchem-1922	73	10	crystal	crystal	NOUN
eurjchem-1922	73	11	structure	structure	NOUN
eurjchem-1922	73	12	is	be	AUX
eurjchem-1922	73	13	shown	show	VERB
eurjchem-1922	73	14	in	in	ADP
eurjchem-1922	73	15	table	table	NOUN
eurjchem-1922	73	16	1	1	NUM
eurjchem-1922	73	17	and	and	CCONJ
eurjchem-1922	73	18	2	2	NUM
eurjchem-1922	73	19	along	along	ADP
eurjchem-1922	73	20	with	with	ADP
eurjchem-1922	73	21	their	their	PRON
eurjchem-1922	73	22	atomic	atomic	ADJ
eurjchem-1922	73	23	coordinates	coordinate	NOUN
eurjchem-1922	73	24	and	and	CCONJ
eurjchem-1922	73	25	displacement	displacement	ADJ
eurjchem-1922	73	26	parameters	parameter	NOUN
eurjchem-1922	73	27	.	.	PUNCT
eurjchem-1922	74	1	the	the	DET
eurjchem-1922	74	2	structural	structural	ADJ
eurjchem-1922	74	3	parameters	parameter	NOUN
eurjchem-1922	74	4	including	include	VERB
eurjchem-1922	74	5	bond	bond	NOUN
eurjchem-1922	74	6	distances	distance	NOUN
eurjchem-1922	74	7	and	and	CCONJ
eurjchem-1922	74	8	bond	bond	NOUN
eurjchem-1922	74	9	angles	angle	NOUN
eurjchem-1922	74	10	for	for	ADP
eurjchem-1922	74	11	compound	compound	NOUN
eurjchem-1922	74	12	3	3	NUM
eurjchem-1922	74	13	are	be	AUX
eurjchem-1922	74	14	listed	list	VERB
eurjchem-1922	74	15	in	in	ADP
eurjchem-1922	74	16	table	table	NOUN
eurjchem-1922	74	17	3	3	NUM
eurjchem-1922	74	18	.	.	PUNCT
eurjchem-1922	75	1	in	in	ADP
eurjchem-1922	75	2	the	the	DET
eurjchem-1922	75	3	crystal	crystal	NOUN
eurjchem-1922	75	4	packing	packing	NOUN
eurjchem-1922	75	5	structure	structure	NOUN
eurjchem-1922	75	6	,	,	PUNCT
eurjchem-1922	75	7	no	no	DET
eurjchem-1922	75	8	significant	significant	ADJ
eurjchem-1922	75	9	hydrogen	hydrogen	NOUN
eurjchem-1922	75	10	bond	bond	NOUN
eurjchem-1922	75	11	was	be	AUX
eurjchem-1922	75	12	found	find	VERB
eurjchem-1922	75	13	.	.	PUNCT
eurjchem-1922	76	1	however	however	ADV
eurjchem-1922	76	2	,	,	PUNCT
eurjchem-1922	76	3	a	a	DET
eurjchem-1922	76	4	short	short	ADJ
eurjchem-1922	76	5	intermolecular	intermolecular	ADJ
eurjchem-1922	76	6	contact	contact	NOUN
eurjchem-1922	76	7	is	be	AUX
eurjchem-1922	76	8	observed	observe	VERB
eurjchem-1922	76	9	between	between	ADP
eurjchem-1922	76	10	o1	o1	NOUN
eurjchem-1922	76	11	and	and	CCONJ
eurjchem-1922	76	12	h6	h6	PROPN
eurjchem-1922	76	13	atoms	atom	NOUN
eurjchem-1922	76	14	.	.	PUNCT
eurjchem-1922	77	1	table	table	NOUN
eurjchem-1922	77	2	1	1	NUM
eurjchem-1922	77	3	.	.	PUNCT
eurjchem-1922	78	1	crystal	crystal	NOUN
eurjchem-1922	78	2	data	datum	NOUN
eurjchem-1922	78	3	and	and	CCONJ
eurjchem-1922	78	4	structure	structure	NOUN
eurjchem-1922	78	5	refinement	refinement	NOUN
eurjchem-1922	78	6	for	for	ADP
eurjchem-1922	78	7	the	the	DET
eurjchem-1922	78	8	title	title	NOUN
eurjchem-1922	78	9	compound	compound	NOUN
eurjchem-1922	78	10	.	.	PUNCT
eurjchem-1922	79	1	parameters	parameter	NOUN
eurjchem-1922	79	2	obtained	obtain	VERB
eurjchem-1922	79	3	specification	specification	NOUN
eurjchem-1922	79	4	ccdc	ccdc	PROPN
eurjchem-1922	79	5	no	no	DET
eurjchem-1922	79	6	194391	194391	NUM
eurjchem-1922	79	7	empirical	empirical	ADJ
eurjchem-1922	79	8	formula	formula	NOUN
eurjchem-1922	79	9	c13h11f6no	c13h11f6no	VERB
eurjchem-1922	79	10	formula	formula	NOUN
eurjchem-1922	79	11	weight	weight	NOUN
eurjchem-1922	79	12	311.23	311.23	NUM
eurjchem-1922	79	13	temperature	temperature	NOUN
eurjchem-1922	79	14	(	(	PUNCT
eurjchem-1922	79	15	k	k	NOUN
eurjchem-1922	79	16	)	)	PUNCT
eurjchem-1922	79	17	293(2	293(2	NUM
eurjchem-1922	79	18	)	)	PUNCT
eurjchem-1922	79	19	crystal	crystal	NOUN
eurjchem-1922	79	20	system	system	NOUN
eurjchem-1922	79	21	monoclinic	monoclinic	ADJ
eurjchem-1922	79	22	space	space	NOUN
eurjchem-1922	79	23	group	group	NOUN
eurjchem-1922	79	24	p21	p21	PROPN
eurjchem-1922	79	25	/	/	SYM
eurjchem-1922	79	26	c	c	PROPN
eurjchem-1922	79	27	a	a	PRON
eurjchem-1922	79	28	(	(	PUNCT
eurjchem-1922	79	29	å	å	NOUN
eurjchem-1922	79	30	)	)	PUNCT
eurjchem-1922	79	31	8.1556(8	8.1556(8	NOUN
eurjchem-1922	79	32	)	)	PUNCT
eurjchem-1922	79	33	b	b	NOUN
eurjchem-1922	79	34	(	(	PUNCT
eurjchem-1922	79	35	å	å	NOUN
eurjchem-1922	79	36	)	)	PUNCT
eurjchem-1922	79	37	24.877(3	24.877(3	NOUN
eurjchem-1922	79	38	)	)	PUNCT
eurjchem-1922	80	1	c	c	NOUN
eurjchem-1922	80	2	(	(	PUNCT
eurjchem-1922	80	3	å	å	NOUN
eurjchem-1922	80	4	)	)	PUNCT
eurjchem-1922	80	5	7.6067(7	7.6067(7	NUM
eurjchem-1922	80	6	)	)	PUNCT
eurjchem-1922	81	1	α	α	PROPN
eurjchem-1922	81	2	(	(	PUNCT
eurjchem-1922	81	3	°	°	PROPN
eurjchem-1922	81	4	)	)	PUNCT
eurjchem-1922	81	5	90	90	NUM
eurjchem-1922	81	6	β	β	X
eurjchem-1922	81	7	(	(	PUNCT
eurjchem-1922	81	8	°	°	NOUN
eurjchem-1922	81	9	)	)	PUNCT
eurjchem-1922	81	10	116.745(6	116.745(6	NOUN
eurjchem-1922	81	11	)	)	PUNCT
eurjchem-1922	81	12	γ	γ	PROPN
eurjchem-1922	81	13	(	(	PUNCT
eurjchem-1922	81	14	°	°	PROPN
eurjchem-1922	81	15	)	)	PUNCT
eurjchem-1922	81	16	90	90	NUM
eurjchem-1922	81	17	volume	volume	NOUN
eurjchem-1922	81	18	(	(	PUNCT
eurjchem-1922	81	19	å3	å3	PROPN
eurjchem-1922	81	20	)	)	PUNCT
eurjchem-1922	81	21	1378.2(3	1378.2(3	NUM
eurjchem-1922	81	22	)	)	PUNCT
eurjchem-1922	81	23	z	z	NOUN
eurjchem-1922	81	24	4	4	NUM
eurjchem-1922	81	25	ρcalc	ρcalc	NOUN
eurjchem-1922	81	26	(	(	PUNCT
eurjchem-1922	81	27	g	g	NOUN
eurjchem-1922	81	28	/	/	SYM
eurjchem-1922	81	29	cm3	cm3	NOUN
eurjchem-1922	81	30	)	)	PUNCT
eurjchem-1922	81	31	1.500	1.500	NUM
eurjchem-1922	81	32	μ	μ	NOUN
eurjchem-1922	81	33	(	(	PUNCT
eurjchem-1922	81	34	mm-1	mm-1	PROPN
eurjchem-1922	81	35	)	)	PUNCT
eurjchem-1922	81	36	0.150	0.150	NUM
eurjchem-1922	81	37	f(000	f(000	NOUN
eurjchem-1922	81	38	)	)	PUNCT
eurjchem-1922	81	39	632.0	632.0	NUM
eurjchem-1922	81	40	radiation	radiation	NOUN
eurjchem-1922	81	41	mokα	mokα	NOUN
eurjchem-1922	81	42	(	(	PUNCT
eurjchem-1922	81	43	λ	λ	X
eurjchem-1922	81	44	=	=	SYM
eurjchem-1922	81	45	0.71073	0.71073	NUM
eurjchem-1922	81	46	)	)	PUNCT
eurjchem-1922	81	47	2θ	2θ	NUM
eurjchem-1922	81	48	range	range	VERB
eurjchem-1922	81	49	for	for	ADP
eurjchem-1922	81	50	data	data	NOUN
eurjchem-1922	81	51	collection	collection	NOUN
eurjchem-1922	81	52	(	(	PUNCT
eurjchem-1922	81	53	°	°	ADP
eurjchem-1922	81	54	)	)	PUNCT
eurjchem-1922	81	55	5.594	5.594	NUM
eurjchem-1922	81	56	to	to	ADP
eurjchem-1922	81	57	56.786	56.786	NUM
eurjchem-1922	81	58	index	index	NOUN
eurjchem-1922	81	59	ranges	range	VERB
eurjchem-1922	81	60	-10	-10	PUNCT
eurjchem-1922	81	61	≤	≤	NUM
eurjchem-1922	81	62	h	h	NOUN
eurjchem-1922	81	63	≤	≤	NUM
eurjchem-1922	81	64	10	10	NUM
eurjchem-1922	81	65	-33	-33	SYM
eurjchem-1922	81	66	≤	≤	NUM
eurjchem-1922	82	1	k	k	X
eurjchem-1922	82	2	≤	≤	NUM
eurjchem-1922	82	3	32	32	NUM
eurjchem-1922	82	4	-10	-10	SYM
eurjchem-1922	82	5	≤	≤	NUM
eurjchem-1922	82	6	l	l	NOUN
eurjchem-1922	82	7	≤	≤	NUM
eurjchem-1922	82	8	10	10	NUM
eurjchem-1922	82	9	reflections	reflection	NOUN
eurjchem-1922	82	10	collected	collect	VERB
eurjchem-1922	82	11	40777	40777	NUM
eurjchem-1922	82	12	independent	independent	ADJ
eurjchem-1922	82	13	reflections	reflection	NOUN
eurjchem-1922	82	14	3413	3413	NUM
eurjchem-1922	83	1	[	[	X
eurjchem-1922	83	2	rint	rint	NOUN
eurjchem-1922	83	3	=	=	SYM
eurjchem-1922	83	4	0.1040	0.1040	NUM
eurjchem-1922	83	5	,	,	PUNCT
eurjchem-1922	83	6	rsigma	rsigma	ADJ
eurjchem-1922	83	7	=	=	SYM
eurjchem-1922	83	8	0.0584	0.0584	NUM
eurjchem-1922	83	9	]	]	PUNCT
eurjchem-1922	83	10	data	data	NOUN
eurjchem-1922	83	11	/	/	SYM
eurjchem-1922	83	12	restraints	restraint	NOUN
eurjchem-1922	83	13	/	/	SYM
eurjchem-1922	83	14	parameters	parameter	NOUN
eurjchem-1922	83	15	3413/0/234	3413/0/234	NUM
eurjchem-1922	83	16	goodness	goodness	NOUN
eurjchem-1922	83	17	-	-	PUNCT
eurjchem-1922	83	18	of	of	ADP
eurjchem-1922	83	19	-	-	PUNCT
eurjchem-1922	83	20	fit	fit	NOUN
eurjchem-1922	83	21	on	on	ADP
eurjchem-1922	83	22	f2	f2	PROPN
eurjchem-1922	83	23	1.051	1.051	NUM
eurjchem-1922	83	24	final	final	ADJ
eurjchem-1922	83	25	r	r	NOUN
eurjchem-1922	83	26	indexes	index	NOUN
eurjchem-1922	83	27	[	[	X
eurjchem-1922	83	28	i≥2σ	i≥2σ	X
eurjchem-1922	83	29	(	(	PUNCT
eurjchem-1922	83	30	i	i	NOUN
eurjchem-1922	83	31	)	)	PUNCT
eurjchem-1922	83	32	]	]	PUNCT
eurjchem-1922	84	1	r1	r1	NOUN
eurjchem-1922	84	2	=	=	PUNCT
eurjchem-1922	84	3	0.0771	0.0771	NUM
eurjchem-1922	84	4	,	,	PUNCT
eurjchem-1922	84	5	wr2	wr2	PROPN
eurjchem-1922	84	6	=	=	PROPN
eurjchem-1922	84	7	0.2062	0.2062	NUM
eurjchem-1922	84	8	final	final	ADJ
eurjchem-1922	84	9	r	r	NOUN
eurjchem-1922	84	10	indexes	index	NOUN
eurjchem-1922	84	11	[	[	X
eurjchem-1922	84	12	all	all	DET
eurjchem-1922	84	13	data	datum	NOUN
eurjchem-1922	84	14	]	]	PUNCT
eurjchem-1922	84	15	r1	r1	NOUN
eurjchem-1922	84	16	=	=	PUNCT
eurjchem-1922	84	17	0.1600	0.1600	PROPN
eurjchem-1922	84	18	,	,	PUNCT
eurjchem-1922	84	19	wr2	wr2	PROPN
eurjchem-1922	84	20	=	=	PROPN
eurjchem-1922	84	21	0.2541	0.2541	NUM
eurjchem-1922	84	22	largest	large	ADJ
eurjchem-1922	84	23	diff	diff	NOUN
eurjchem-1922	84	24	.	.	PUNCT
eurjchem-1922	84	25	peak	peak	PROPN
eurjchem-1922	84	26	/	/	SYM
eurjchem-1922	84	27	hole	hole	NOUN
eurjchem-1922	84	28	(	(	PUNCT
eurjchem-1922	84	29	e.å-3	e.å-3	PROPN
eurjchem-1922	84	30	)	)	PUNCT
eurjchem-1922	84	31	0.40/-0.37	0.40/-0.37	PROPN
eurjchem-1922	84	32	(	(	PUNCT
eurjchem-1922	84	33	a	a	NOUN
eurjchem-1922	84	34	)	)	PUNCT
eurjchem-1922	84	35	(	(	PUNCT
eurjchem-1922	84	36	b	b	X
eurjchem-1922	84	37	)	)	PUNCT
eurjchem-1922	84	38	figure	figure	NOUN
eurjchem-1922	84	39	2	2	NUM
eurjchem-1922	84	40	.	.	PUNCT
eurjchem-1922	84	41	(	(	PUNCT
eurjchem-1922	84	42	a	a	X
eurjchem-1922	84	43	)	)	PUNCT
eurjchem-1922	84	44	packing	packing	NOUN
eurjchem-1922	84	45	of	of	ADP
eurjchem-1922	84	46	the	the	DET
eurjchem-1922	84	47	crystal	crystal	NOUN
eurjchem-1922	84	48	in	in	ADP
eurjchem-1922	84	49	three	three	NUM
eurjchem-1922	84	50	-	-	PUNCT
eurjchem-1922	84	51	dimensional	dimensional	ADJ
eurjchem-1922	84	52	lattice	lattice	NOUN
eurjchem-1922	84	53	,	,	PUNCT
eurjchem-1922	84	54	(	(	PUNCT
eurjchem-1922	84	55	b	b	X
eurjchem-1922	84	56	)	)	PUNCT
eurjchem-1922	84	57	short	short	ADJ
eurjchem-1922	84	58	contact	contact	NOUN
eurjchem-1922	84	59	formed	form	VERB
eurjchem-1922	84	60	between	between	ADP
eurjchem-1922	84	61	oxygen	oxygen	NOUN
eurjchem-1922	84	62	and	and	CCONJ
eurjchem-1922	84	63	hydrogen	hydrogen	NOUN
eurjchem-1922	84	64	.	.	PUNCT
eurjchem-1922	85	1	4	4	X
eurjchem-1922	85	2	.	.	X
eurjchem-1922	85	3	conclusion	conclusion	NOUN
eurjchem-1922	85	4	in	in	ADP
eurjchem-1922	85	5	this	this	DET
eurjchem-1922	85	6	article	article	NOUN
eurjchem-1922	85	7	,	,	PUNCT
eurjchem-1922	85	8	we	we	PRON
eurjchem-1922	85	9	report	report	VERB
eurjchem-1922	85	10	the	the	DET
eurjchem-1922	85	11	successful	successful	ADJ
eurjchem-1922	85	12	synthesis	synthesis	NOUN
eurjchem-1922	85	13	of	of	ADP
eurjchem-1922	85	14	a	a	DET
eurjchem-1922	85	15	new	new	ADJ
eurjchem-1922	85	16	enaminone	enaminone	NOUN
eurjchem-1922	85	17	,	,	PUNCT
eurjchem-1922	85	18	which	which	PRON
eurjchem-1922	85	19	may	may	AUX
eurjchem-1922	85	20	act	act	VERB
eurjchem-1922	85	21	as	as	ADP
eurjchem-1922	85	22	a	a	DET
eurjchem-1922	85	23	building	building	NOUN
eurjchem-1922	85	24	block	block	NOUN
eurjchem-1922	85	25	for	for	ADP
eurjchem-1922	85	26	numerous	numerous	ADJ
eurjchem-1922	85	27	hitherto	hitherto	NOUN
eurjchem-1922	85	28	unreported	unreported	ADJ
eurjchem-1922	85	29	novel	novel	ADJ
eurjchem-1922	85	30	molecules	molecule	NOUN
eurjchem-1922	85	31	.	.	PUNCT
eurjchem-1922	86	1	its	its	PRON
eurjchem-1922	86	2	spectral	spectral	ADJ
eurjchem-1922	86	3	characterization	characterization	NOUN
eurjchem-1922	86	4	has	have	AUX
eurjchem-1922	86	5	been	be	AUX
eurjchem-1922	86	6	studied	study	VERB
eurjchem-1922	86	7	.	.	PUNCT
eurjchem-1922	87	1	its	its	PRON
eurjchem-1922	87	2	crystalline	crystalline	ADJ
eurjchem-1922	87	3	characterization	characterization	NOUN
eurjchem-1922	87	4	shows	show	VERB
eurjchem-1922	87	5	that	that	SCONJ
eurjchem-1922	87	6	it	it	PRON
eurjchem-1922	87	7	adopts	adopt	VERB
eurjchem-1922	87	8	trans	tran	NOUN
eurjchem-1922	87	9	-	-	NOUN
eurjchem-1922	87	10	configuration	configuration	NOUN
eurjchem-1922	87	11	.	.	PUNCT
eurjchem-1922	88	1	the	the	DET
eurjchem-1922	88	2	bond	bond	NOUN
eurjchem-1922	88	3	angles	angle	NOUN
eurjchem-1922	88	4	of	of	ADP
eurjchem-1922	88	5	c1	c1	PROPN
eurjchem-1922	88	6	-	-	PUNCT
eurjchem-1922	88	7	c7	c7	PROPN
eurjchem-1922	88	8	-	-	PUNCT
eurjchem-1922	88	9	c8	c8	PROPN
eurjchem-1922	88	10	,	,	PUNCT
eurjchem-1922	88	11	c7	c7	PROPN
eurjchem-1922	88	12	-	-	PUNCT
eurjchem-1922	88	13	c8	c8	PROPN
eurjchem-1922	88	14	-	-	PUNCT
eurjchem-1922	88	15	c9	c9	PROPN
eurjchem-1922	88	16	and	and	CCONJ
eurjchem-1922	88	17	c8	c8	PROPN
eurjchem-1922	88	18	-	-	PUNCT
eurjchem-1922	88	19	c9	c9	NOUN
eurjchem-1922	88	20	-	-	PUNCT
eurjchem-1922	88	21	n1	n1	NOUN
eurjchem-1922	88	22	are	be	AUX
eurjchem-1922	88	23	found	find	VERB
eurjchem-1922	88	24	to	to	PART
eurjchem-1922	88	25	be	be	AUX
eurjchem-1922	88	26	118.4(3	118.4(3	NUM
eurjchem-1922	88	27	)	)	PUNCT
eurjchem-1922	88	28	°	°	PROPN
eurjchem-1922	88	29	,	,	PUNCT
eurjchem-1922	88	30	119.8(3	119.8(3	NUM
eurjchem-1922	88	31	)	)	PUNCT
eurjchem-1922	88	32	°	°	PROPN
eurjchem-1922	88	33	,	,	PUNCT
eurjchem-1922	88	34	and	and	CCONJ
eurjchem-1922	88	35	128.2(3	128.2(3	NUM
eurjchem-1922	88	36	)	)	PUNCT
eurjchem-1922	88	37	°	°	NOUN
eurjchem-1922	88	38	,	,	PUNCT
eurjchem-1922	88	39	respectively	respectively	ADV
eurjchem-1922	88	40	.	.	PUNCT
eurjchem-1922	89	1	these	these	PRON
eurjchem-1922	89	2	obtained	obtain	VERB
eurjchem-1922	89	3	values	value	NOUN
eurjchem-1922	89	4	suggested	suggest	VERB
eurjchem-1922	89	5	that	that	SCONJ
eurjchem-1922	89	6	a	a	DET
eurjchem-1922	89	7	planer	planer	NOUN
eurjchem-1922	89	8	structure	structure	NOUN
eurjchem-1922	89	9	in	in	ADP
eurjchem-1922	89	10	the	the	DET
eurjchem-1922	89	11	molecule	molecule	NOUN
eurjchem-1922	89	12	.	.	PUNCT
eurjchem-1922	90	1	2019	2019	NUM
eurjchem-1922	90	2	–	–	PUNCT
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eurjchem-1922	95	109	)	)	PUNCT
eurjchem-1922	95	110	c13	c13	PROPN
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eurjchem-1922	95	112	f2	f2	PROPN
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eurjchem-1922	95	114	)	)	PUNCT
eurjchem-1922	95	115	n1	n1	NOUN
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eurjchem-1922	95	117	c11	c11	NOUN
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eurjchem-1922	95	119	)	)	PUNCT
eurjchem-1922	95	120	c13	c13	NOUN
eurjchem-1922	95	121	-	-	PUNCT
eurjchem-1922	95	122	f3	f3	ADJ
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eurjchem-1922	95	124	)	)	PUNCT
eurjchem-1922	95	125	n1	n1	PROPN
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eurjchem-1922	95	127	c10	c10	VERB
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eurjchem-1922	95	129	)	)	PUNCT
eurjchem-1922	95	130	atom	atom	NOUN
eurjchem-1922	95	131	-	-	PUNCT
eurjchem-1922	95	132	atom	atom	NOUN
eurjchem-1922	95	133	-	-	PUNCT
eurjchem-1922	95	134	atom	atom	NOUN
eurjchem-1922	95	135	bond	bond	NOUN
eurjchem-1922	95	136	angles	angle	NOUN
eurjchem-1922	95	137	(	(	PUNCT
eurjchem-1922	95	138	°	°	NOUN
eurjchem-1922	95	139	)	)	PUNCT
eurjchem-1922	95	140	atom	atom	NOUN
eurjchem-1922	95	141	-	-	PUNCT
eurjchem-1922	95	142	atom	atom	NOUN
eurjchem-1922	95	143	-	-	PUNCT
eurjchem-1922	95	144	atom	atom	NOUN
eurjchem-1922	95	145	bond	bond	NOUN
eurjchem-1922	95	146	angles	angle	NOUN
eurjchem-1922	95	147	(	(	PUNCT
eurjchem-1922	95	148	°	°	PRON
eurjchem-1922	95	149	)	)	PUNCT
eurjchem-1922	95	150	c9	c9	NOUN
eurjchem-1922	95	151	-	-	PUNCT
eurjchem-1922	95	152	c8	c8	PROPN
eurjchem-1922	95	153	-	-	PUNCT
eurjchem-1922	95	154	c7	c7	PROPN
eurjchem-1922	95	155	119.8(3	119.8(3	PROPN
eurjchem-1922	95	156	)	)	PUNCT
eurjchem-1922	95	157	c6	c6	PROPN
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eurjchem-1922	95	159	c5	c5	PROPN
eurjchem-1922	95	160	-	-	PUNCT
eurjchem-1922	95	161	c12	c12	PROPN
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eurjchem-1922	95	163	)	)	PUNCT
eurjchem-1922	95	164	c3	c3	PROPN
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eurjchem-1922	95	166	c2	c2	PROPN
eurjchem-1922	95	167	-	-	PUNCT
eurjchem-1922	95	168	c1	c1	PROPN
eurjchem-1922	95	169	120.4(3	120.4(3	NUM
eurjchem-1922	95	170	)	)	PUNCT
eurjchem-1922	95	171	c4	c4	NOUN
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eurjchem-1922	95	173	c5	c5	PROPN
eurjchem-1922	95	174	-	-	PUNCT
eurjchem-1922	95	175	c6	c6	PROPN
eurjchem-1922	95	176	120.5(3	120.5(3	NUM
eurjchem-1922	95	177	)	)	PUNCT
eurjchem-1922	95	178	n1	n1	NOUN
eurjchem-1922	95	179	-	-	PUNCT
eurjchem-1922	95	180	c9	c9	NOUN
eurjchem-1922	95	181	-	-	PUNCT
eurjchem-1922	95	182	c8	c8	PROPN
eurjchem-1922	95	183	128.2(3	128.2(3	NUM
eurjchem-1922	95	184	)	)	PUNCT
eurjchem-1922	95	185	c4	c4	NOUN
eurjchem-1922	95	186	-	-	PUNCT
eurjchem-1922	95	187	c5	c5	PROPN
eurjchem-1922	95	188	-	-	PUNCT
eurjchem-1922	95	189	c12	c12	PROPN
eurjchem-1922	95	190	119.3(3	119.3(3	NUM
eurjchem-1922	95	191	)	)	PUNCT
eurjchem-1922	95	192	o1	o1	PROPN
eurjchem-1922	95	193	-	-	PUNCT
eurjchem-1922	95	194	c7	c7	PROPN
eurjchem-1922	95	195	-	-	PUNCT
eurjchem-1922	95	196	c8	c8	PROPN
eurjchem-1922	95	197	124.1(3	124.1(3	NUM
eurjchem-1922	95	198	)	)	PUNCT
eurjchem-1922	95	199	c5	c5	PROPN
eurjchem-1922	95	200	-	-	PUNCT
eurjchem-1922	95	201	c4	c4	NOUN
eurjchem-1922	95	202	-	-	PUNCT
eurjchem-1922	95	203	c3	c3	NOUN
eurjchem-1922	95	204	119.0(3	119.0(3	NOUN
eurjchem-1922	95	205	)	)	PUNCT
eurjchem-1922	95	206	o1	o1	NOUN
eurjchem-1922	95	207	-	-	PUNCT
eurjchem-1922	95	208	c7	c7	NOUN
eurjchem-1922	95	209	-	-	PUNCT
eurjchem-1922	95	210	c1	c1	PROPN
eurjchem-1922	95	211	117.5(3	117.5(3	NUM
eurjchem-1922	95	212	)	)	PUNCT
eurjchem-1922	95	213	f4	f4	PROPN
eurjchem-1922	95	214	-	-	PUNCT
eurjchem-1922	95	215	c12	c12	NOUN
eurjchem-1922	95	216	-	-	PUNCT
eurjchem-1922	95	217	c5	c5	PROPN
eurjchem-1922	95	218	114.3(3	114.3(3	NUM
eurjchem-1922	95	219	)	)	PUNCT
eurjchem-1922	95	220	c8	c8	PROPN
eurjchem-1922	95	221	-	-	PUNCT
eurjchem-1922	95	222	c7	c7	PROPN
eurjchem-1922	95	223	-	-	PUNCT
eurjchem-1922	95	224	c1	c1	PROPN
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eurjchem-1922	95	226	)	)	PUNCT
eurjchem-1922	95	227	f4	f4	PROPN
eurjchem-1922	95	228	-	-	PUNCT
eurjchem-1922	95	229	c12	c12	NOUN
eurjchem-1922	95	230	-	-	PUNCT
eurjchem-1922	95	231	f6	f6	NOUN
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eurjchem-1922	95	233	)	)	PUNCT
eurjchem-1922	95	234	c2	c2	PROPN
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eurjchem-1922	95	236	c1	c1	PROPN
eurjchem-1922	95	237	-	-	PUNCT
eurjchem-1922	95	238	c7	c7	PROPN
eurjchem-1922	95	239	118.3(3	118.3(3	NUM
eurjchem-1922	95	240	)	)	PUNCT
eurjchem-1922	95	241	f5	f5	PROPN
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eurjchem-1922	95	243	c12	c12	NOUN
eurjchem-1922	95	244	-	-	PUNCT
eurjchem-1922	95	245	c5	c5	PROPN
eurjchem-1922	95	246	113.3(4	113.3(4	NUM
eurjchem-1922	95	247	)	)	PUNCT
eurjchem-1922	95	248	c6	c6	PROPN
eurjchem-1922	95	249	-	-	PUNCT
eurjchem-1922	95	250	c1	c1	PROPN
eurjchem-1922	95	251	-	-	PUNCT
eurjchem-1922	95	252	c2	c2	PROPN
eurjchem-1922	95	253	119.0(3	119.0(3	NUM
eurjchem-1922	95	254	)	)	PUNCT
eurjchem-1922	95	255	f5	f5	PROPN
eurjchem-1922	95	256	-	-	PUNCT
eurjchem-1922	95	257	c12	c12	NOUN
eurjchem-1922	95	258	-	-	PUNCT
eurjchem-1922	95	259	f4	f4	NOUN
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eurjchem-1922	95	261	)	)	PUNCT
eurjchem-1922	95	262	c6	c6	PROPN
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eurjchem-1922	95	264	c1	c1	PROPN
eurjchem-1922	95	265	-	-	PUNCT
eurjchem-1922	95	266	c7	c7	PROPN
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eurjchem-1922	95	268	)	)	PUNCT
eurjchem-1922	95	269	f5	f5	PROPN
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eurjchem-1922	95	271	c12	c12	NOUN
eurjchem-1922	95	272	-	-	PUNCT
eurjchem-1922	95	273	f6	f6	NOUN
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eurjchem-1922	95	275	)	)	PUNCT
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eurjchem-1922	95	277	-	-	PUNCT
eurjchem-1922	95	278	c6	c6	PROPN
eurjchem-1922	95	279	-	-	PUNCT
eurjchem-1922	95	280	c5	c5	PROPN
eurjchem-1922	95	281	120.3(3	120.3(3	NUM
eurjchem-1922	95	282	)	)	PUNCT
eurjchem-1922	95	283	f6	f6	PROPN
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eurjchem-1922	95	285	c12	c12	NOUN
eurjchem-1922	95	286	-	-	PUNCT
eurjchem-1922	95	287	c5	c5	PROPN
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eurjchem-1922	95	289	)	)	PUNCT
eurjchem-1922	95	290	c9	c9	NOUN
eurjchem-1922	95	291	-	-	PUNCT
eurjchem-1922	95	292	n1	n1	NOUN
eurjchem-1922	95	293	-	-	PUNCT
eurjchem-1922	95	294	c11	c11	NOUN
eurjchem-1922	95	295	121.2(3	121.2(3	NUM
eurjchem-1922	95	296	)	)	PUNCT
eurjchem-1922	95	297	f1	f1	NOUN
eurjchem-1922	95	298	-	-	PUNCT
eurjchem-1922	95	299	c13	c13	NOUN
eurjchem-1922	95	300	-	-	PUNCT
eurjchem-1922	95	301	c3	c3	PROPN
eurjchem-1922	95	302	115.2(4	115.2(4	NUM
eurjchem-1922	95	303	)	)	PUNCT
eurjchem-1922	95	304	c9	c9	NOUN
eurjchem-1922	95	305	-	-	PUNCT
eurjchem-1922	95	306	n1	n1	NOUN
eurjchem-1922	95	307	-	-	PUNCT
eurjchem-1922	95	308	c10	c10	VERB
eurjchem-1922	95	309	120.9(3	120.9(3	NUM
eurjchem-1922	95	310	)	)	PUNCT
eurjchem-1922	95	311	f1	f1	NOUN
eurjchem-1922	95	312	-	-	PUNCT
eurjchem-1922	95	313	c13	c13	NOUN
eurjchem-1922	95	314	-	-	PUNCT
eurjchem-1922	95	315	f2	f2	PROPN
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eurjchem-1922	95	317	)	)	PUNCT
eurjchem-1922	95	318	c11	c11	NOUN
eurjchem-1922	95	319	-	-	PUNCT
eurjchem-1922	95	320	n1	n1	NOUN
eurjchem-1922	95	321	-	-	PUNCT
eurjchem-1922	95	322	c10	c10	VERB
eurjchem-1922	95	323	117.8(4	117.8(4	NUM
eurjchem-1922	95	324	)	)	PUNCT
eurjchem-1922	95	325	f1	f1	NOUN
eurjchem-1922	95	326	-	-	PUNCT
eurjchem-1922	95	327	c13	c13	NOUN
eurjchem-1922	95	328	-	-	PUNCT
eurjchem-1922	95	329	f3	f3	PROPN
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eurjchem-1922	95	331	)	)	PUNCT
eurjchem-1922	95	332	c2	c2	PROPN
eurjchem-1922	95	333	-	-	PUNCT
eurjchem-1922	95	334	c3	c3	PROPN
eurjchem-1922	95	335	-	-	PUNCT
eurjchem-1922	95	336	c4	c4	ADJ
eurjchem-1922	95	337	120.7(3	120.7(3	NUM
eurjchem-1922	95	338	)	)	PUNCT
eurjchem-1922	95	339	f2	f2	PROPN
eurjchem-1922	95	340	-	-	PUNCT
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eurjchem-1922	95	342	-	-	PUNCT
eurjchem-1922	95	343	c3	c3	PROPN
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eurjchem-1922	95	345	)	)	PUNCT
eurjchem-1922	95	346	c2	c2	PROPN
eurjchem-1922	95	347	-	-	PUNCT
eurjchem-1922	95	348	c3	c3	PROPN
eurjchem-1922	95	349	-	-	PROPN
eurjchem-1922	95	350	c13	c13	PROPN
eurjchem-1922	95	351	119.3(4	119.3(4	NOUN
eurjchem-1922	95	352	)	)	PUNCT
eurjchem-1922	95	353	f2	f2	PROPN
eurjchem-1922	95	354	-	-	PUNCT
eurjchem-1922	95	355	c13	c13	NOUN
eurjchem-1922	95	356	-	-	PUNCT
eurjchem-1922	95	357	f3	f3	ADJ
eurjchem-1922	95	358	102.9(5	102.9(5	NUM
eurjchem-1922	95	359	)	)	PUNCT
eurjchem-1922	95	360	c4	c4	NOUN
eurjchem-1922	95	361	-	-	PUNCT
eurjchem-1922	95	362	c3	c3	NOUN
eurjchem-1922	95	363	-	-	PROPN
eurjchem-1922	95	364	c13	c13	PROPN
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eurjchem-1922	95	366	)	)	PUNCT
eurjchem-1922	95	367	f3	f3	PROPN
eurjchem-1922	95	368	-	-	PUNCT
eurjchem-1922	95	369	c13	c13	NOUN
eurjchem-1922	95	370	-	-	PUNCT
eurjchem-1922	95	371	c3	c3	PROPN
eurjchem-1922	95	372	112.8(4	112.8(4	NUM
eurjchem-1922	95	373	)	)	PUNCT
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eurjchem-1922	95	375	the	the	DET
eurjchem-1922	95	376	authors	author	NOUN
eurjchem-1922	95	377	would	would	AUX
eurjchem-1922	95	378	like	like	VERB
eurjchem-1922	95	379	to	to	PART
eurjchem-1922	95	380	thank	thank	VERB
eurjchem-1922	95	381	rev	rev	PROPN
eurjchem-1922	95	382	.	.	PUNCT
eurjchem-1922	96	1	fr	fr	PROPN
eurjchem-1922	96	2	.	.	PUNCT
eurjchem-1922	97	1	dr	dr	PROPN
eurjchem-1922	97	2	.	.	PROPN
eurjchem-1922	97	3	stephen	stephen	PROPN
eurjchem-1922	97	4	mavely	mavely	PROPN
eurjchem-1922	97	5	,	,	PUNCT
eurjchem-1922	97	6	vice	vice	NOUN
eurjchem-1922	97	7	chancellor	chancellor	NOUN
eurjchem-1922	97	8	,	,	PUNCT
eurjchem-1922	97	9	assam	assam	PROPN
eurjchem-1922	97	10	don	don	PROPN
eurjchem-1922	97	11	bosco	bosco	PROPN
eurjchem-1922	97	12	university	university	PROPN
eurjchem-1922	97	13	for	for	ADP
eurjchem-1922	97	14	providing	provide	VERB
eurjchem-1922	97	15	infrastructure	infrastructure	NOUN
eurjchem-1922	97	16	for	for	ADP
eurjchem-1922	97	17	the	the	DET
eurjchem-1922	97	18	execution	execution	NOUN
eurjchem-1922	97	19	of	of	ADP
eurjchem-1922	97	20	this	this	DET
eurjchem-1922	97	21	work	work	NOUN
eurjchem-1922	97	22	.	.	PUNCT
eurjchem-1922	98	1	the	the	DET
eurjchem-1922	98	2	authors	author	NOUN
eurjchem-1922	98	3	also	also	ADV
eurjchem-1922	98	4	express	express	VERB
eurjchem-1922	98	5	their	their	PRON
eurjchem-1922	98	6	heart	heart	NOUN
eurjchem-1922	98	7	-	-	PUNCT
eurjchem-1922	98	8	full	full	ADJ
eurjchem-1922	98	9	gratitude	gratitude	NOUN
eurjchem-1922	98	10	to	to	ADP
eurjchem-1922	98	11	mr	mr	PROPN
eurjchem-1922	98	12	.	.	PROPN
eurjchem-1922	98	13	tridib	tridib	PROPN
eurjchem-1922	98	14	ranjan	ranjan	PROPN
eurjchem-1922	98	15	nath	nath	PROPN
eurjchem-1922	98	16	and	and	CCONJ
eurjchem-1922	98	17	mr	mr	PROPN
eurjchem-1922	98	18	.	.	PROPN
eurjchem-1922	98	19	biraj	biraj	PROPN
eurjchem-1922	98	20	jyoti	jyoti	PROPN
eurjchem-1922	98	21	borah	borah	PROPN
eurjchem-1922	98	22	,	,	PUNCT
eurjchem-1922	98	23	saic	saic	PROPN
eurjchem-1922	98	24	,	,	PUNCT
eurjchem-1922	98	25	tezpur	tezpur	PROPN
eurjchem-1922	98	26	university	university	PROPN
eurjchem-1922	98	27	,	,	PUNCT
eurjchem-1922	98	28	napaam	napaam	NOUN
eurjchem-1922	98	29	for	for	ADP
eurjchem-1922	98	30	recording	record	VERB
eurjchem-1922	98	31	the	the	DET
eurjchem-1922	98	32	xrd	xrd	PROPN
eurjchem-1922	98	33	spectra	spectra	PROPN
eurjchem-1922	98	34	.	.	PUNCT
eurjchem-1922	99	1	the	the	DET
eurjchem-1922	99	2	authors	author	NOUN
eurjchem-1922	99	3	are	be	AUX
eurjchem-1922	99	4	very	very	ADV
eurjchem-1922	99	5	much	much	ADV
eurjchem-1922	99	6	grateful	grateful	ADJ
eurjchem-1922	99	7	to	to	ADP
eurjchem-1922	99	8	mr	mr	PROPN
eurjchem-1922	99	9	.	.	PROPN
eurjchem-1922	99	10	farlando	farlando	PROPN
eurjchem-1922	99	11	diengdoh	diengdoh	PROPN
eurjchem-1922	99	12	,	,	PUNCT
eurjchem-1922	99	13	department	department	NOUN
eurjchem-1922	99	14	of	of	ADP
eurjchem-1922	99	15	chemistry	chemistry	PROPN
eurjchem-1922	99	16	,	,	PUNCT
eurjchem-1922	99	17	st	st	PROPN
eurjchem-1922	99	18	.	.	PROPN
eurjchem-1922	99	19	anthony	anthony	PROPN
eurjchem-1922	99	20	’s	’s	PART
eurjchem-1922	99	21	college	college	PROPN
eurjchem-1922	99	22	,	,	PUNCT
eurjchem-1922	99	23	shillong	shillong	PROPN
eurjchem-1922	99	24	for	for	ADP
eurjchem-1922	99	25	his	his	PRON
eurjchem-1922	99	26	generous	generous	ADJ
eurjchem-1922	99	27	help	help	NOUN
eurjchem-1922	99	28	extended	extend	VERB
eurjchem-1922	99	29	for	for	ADP
eurjchem-1922	99	30	solving	solve	VERB
eurjchem-1922	99	31	the	the	DET
eurjchem-1922	99	32	xrd	xrd	PROPN
eurjchem-1922	99	33	spectra	spectra	PROPN
eurjchem-1922	99	34	.	.	PUNCT
eurjchem-1922	100	1	supporting	support	VERB
eurjchem-1922	100	2	information	information	NOUN
eurjchem-1922	100	3	ccdc-194391	ccdc-194391	NOUN
eurjchem-1922	100	4	contains	contain	VERB
eurjchem-1922	100	5	the	the	DET
eurjchem-1922	100	6	supplementary	supplementary	ADJ
eurjchem-1922	100	7	crystallographic	crystallographic	ADJ
eurjchem-1922	100	8	data	datum	NOUN
eurjchem-1922	100	9	for	for	ADP
eurjchem-1922	100	10	this	this	DET
eurjchem-1922	100	11	paper	paper	NOUN
eurjchem-1922	100	12	.	.	PUNCT
eurjchem-1922	101	1	these	these	DET
eurjchem-1922	101	2	data	datum	NOUN
eurjchem-1922	101	3	can	can	AUX
eurjchem-1922	101	4	be	be	AUX
eurjchem-1922	101	5	obtained	obtain	VERB
eurjchem-1922	101	6	free	free	ADJ
eurjchem-1922	101	7	of	of	ADP
eurjchem-1922	101	8	charge	charge	NOUN
eurjchem-1922	101	9	via	via	ADP
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eurjchem-1922	108	40	(	(	PUNCT
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eurjchem-1922	111	6	-	-	SYM
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eurjchem-1922	152	31	.	.	PUNCT
eurjchem-1922	153	1	instrumentation	instrumentation	NOUN
eurjchem-1922	153	2	2.2	2.2	NUM
eurjchem-1922	153	3	.	.	PUNCT
eurjchem-1922	154	1	synthesis	synthesis	VERB
eurjchem-1922	154	2	2.3	2.3	NUM
eurjchem-1922	154	3	.	.	PUNCT
eurjchem-1922	155	1	crystallographic	crystallographic	ADJ
eurjchem-1922	155	2	details	detail	NOUN
eurjchem-1922	155	3	3	3	NUM
eurjchem-1922	155	4	.	.	NOUN
eurjchem-1922	155	5	results	result	NOUN
eurjchem-1922	155	6	and	and	CCONJ
eurjchem-1922	155	7	discussion	discussion	NOUN
eurjchem-1922	155	8	3.1	3.1	NUM
eurjchem-1922	155	9	.	.	PUNCT
eurjchem-1922	156	1	spectral	spectral	ADJ
eurjchem-1922	156	2	analysis	analysis	NOUN
eurjchem-1922	156	3	3.2	3.2	NUM
eurjchem-1922	156	4	.	.	PUNCT
eurjchem-1922	157	1	crystal	crystal	NOUN
eurjchem-1922	157	2	structure	structure	NOUN
eurjchem-1922	157	3	4	4	NUM
eurjchem-1922	157	4	.	.	PUNCT
eurjchem-1922	158	1	conclusion	conclusion	NOUN
eurjchem-1922	158	2	acknowledgements	acknowledgement	NOUN
eurjchem-1922	158	3	supporting	support	VERB
eurjchem-1922	158	4	information	information	NOUN
eurjchem-1922	158	5	disclosure	disclosure	NOUN
eurjchem-1922	158	6	statement	statement	NOUN
eurjchem-1922	158	7	funding	fund	VERB
eurjchem-1922	158	8	orcid	orcid	PROPN
eurjchem-1922	158	9	references	reference	NOUN
eurjchem-1922	158	10	printfield10	printfield10	NOUN
eurjchem-1922	158	11	:	:	PUNCT
eurjchem-1922	158	12	printfield11	printfield11	NOUN
eurjchem-1922	158	13	:	:	PUNCT
eurjchem-1922	158	14	printfield12	printfield12	PROPN
eurjchem-1922	158	15	:	:	PUNCT
eurjchem-1922	158	16	printfield13	printfield13	VERB
eurjchem-1922	158	17	:	:	PUNCT
eurjchem-1922	158	18	printfield14	printfield14	NOUN
eurjchem-1922	158	19	:	:	PUNCT
eurjchem-1922	158	20	printfield20	printfield20	PROPN
eurjchem-1922	158	21	:	:	PUNCT
eurjchem-1922	159	1	printfield21	printfield21	ADJ
eurjchem-1922	159	2	:	:	PUNCT
eurjchem-1922	159	3	printfield22	printfield22	NOUN
eurjchem-1922	159	4	:	:	PUNCT
eurjchem-1922	159	5	printfield23	printfield23	NOUN
eurjchem-1922	159	6	:	:	PUNCT
eurjchem-1922	159	7	printfield24	printfield24	NOUN
eurjchem-1922	159	8	:	:	PUNCT