id	sid	tid	token	lemma	pos
eurjchem-193	1	1	untitled	untitle	VERB
eurjchem-193	1	2	european	european	PROPN
eurjchem-193	1	3	journal	journal	PROPN
eurjchem-193	1	4	of	of	ADP
eurjchem-193	1	5	chemistry	chemistry	NOUN
eurjchem-193	1	6	2	2	NUM
eurjchem-193	1	7	(	(	PUNCT
eurjchem-193	1	8	4	4	NUM
eurjchem-193	1	9	)	)	PUNCT
eurjchem-193	1	10	(	(	PUNCT
eurjchem-193	1	11	2011	2011	NUM
eurjchem-193	1	12	)	)	PUNCT
eurjchem-193	1	13	475‐479	475‐479	NUM
eurjchem-193	1	14	european	european	ADJ
eurjchem-193	1	15	journal	journal	PROPN
eurjchem-193	1	16	of	of	ADP
eurjchem-193	1	17	chemistry	chemistry	NOUN
eurjchem-193	1	18	issn	issn	PROPN
eurjchem-193	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-193	1	20	(	(	PUNCT
eurjchem-193	1	21	print	print	NOUN
eurjchem-193	1	22	)	)	PUNCT
eurjchem-193	1	23	/	/	SYM
eurjchem-193	1	24	issn	issn	PROPN
eurjchem-193	1	25	2153‐2257	2153‐2257	NUM
eurjchem-193	1	26	(	(	PUNCT
eurjchem-193	1	27	online	online	ADJ
eurjchem-193	1	28	)	)	PUNCT
eurjchem-193	1	29			NOUN
eurjchem-193	1	30	2011	2011	NUM
eurjchem-193	1	31	eurjchem	eurjchem	PROPN
eurjchem-193	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-193	1	33	/	/	SYM
eurjchem-193	1	34	eurjchem.2.4.475‐479.193	eurjchem.2.4.475‐479.193	NOUN
eurjchem-193	1	35	european	european	ADJ
eurjchem-193	1	36	journal	journal	PROPN
eurjchem-193	1	37	of	of	ADP
eurjchem-193	1	38	chemistry	chemistry	PROPN
eurjchem-193	1	39	journal	journal	PROPN
eurjchem-193	1	40	homepage	homepage	NOUN
eurjchem-193	1	41	:	:	PUNCT
eurjchem-193	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-193	1	43	synthesis	synthesis	NOUN
eurjchem-193	1	44	and	and	CCONJ
eurjchem-193	1	45	reactions	reaction	NOUN
eurjchem-193	1	46	of	of	ADP
eurjchem-193	1	47	(	(	PUNCT
eurjchem-193	1	48	z)‐2‐imino‐5‐(3,4,5‐trimethoxy	z)‐2‐imino‐5‐(3,4,5‐trimethoxy	PROPN
eurjchem-193	1	49	benzylidene)thiazolidin‐4(h)one	benzylidene)thiazolidin‐4(h)one	PROPN
eurjchem-193	1	50	mahmoud	mahmoud	PROPN
eurjchem-193	1	51	refaee	refaee	PROPN
eurjchem-193	1	52	mahmoud	mahmoud	PROPN
eurjchem-193	1	53	*	*	PROPN
eurjchem-193	1	54	,	,	PUNCT
eurjchem-193	1	55	hassan	hassan	PROPN
eurjchem-193	1	56	mohamed	mohamed	PROPN
eurjchem-193	1	57	fawzy	fawzy	PROPN
eurjchem-193	1	58	madkour	madkour	PROPN
eurjchem-193	1	59	,	,	PUNCT
eurjchem-193	1	60	eman	eman	PROPN
eurjchem-193	1	61	abd	abd	PROPN
eurjchem-193	1	62	el‐fattah	el‐fattah	PROPN
eurjchem-193	1	63	el‐bordany	el‐bordany	PROPN
eurjchem-193	1	64	and	and	CCONJ
eurjchem-193	1	65	el‐sayed	el‐saye	VERB
eurjchem-193	1	66	ahmed	ahmed	PROPN
eurjchem-193	1	67	soliman	soliman	PROPN
eurjchem-193	1	68	chemistry	chemistry	PROPN
eurjchem-193	1	69	department	department	PROPN
eurjchem-193	1	70	,	,	PUNCT
eurjchem-193	1	71	faculty	faculty	NOUN
eurjchem-193	1	72	of	of	ADP
eurjchem-193	1	73	science	science	NOUN
eurjchem-193	1	74	,	,	PUNCT
eurjchem-193	1	75	ain	ain	PROPN
eurjchem-193	1	76	shams	shams	PROPN
eurjchem-193	1	77	university	university	PROPN
eurjchem-193	1	78	,	,	PUNCT
eurjchem-193	1	79	cairo	cairo	PROPN
eurjchem-193	1	80	,	,	PUNCT
eurjchem-193	1	81	11566	11566	NUM
eurjchem-193	1	82	,	,	PUNCT
eurjchem-193	1	83	egypt	egypt	PROPN
eurjchem-193	1	84	*	*	PUNCT
eurjchem-193	1	85	corresponding	correspond	VERB
eurjchem-193	1	86	author	author	NOUN
eurjchem-193	1	87	at	at	ADP
eurjchem-193	1	88	:	:	PUNCT
eurjchem-193	1	89	chemistry	chemistry	NOUN
eurjchem-193	1	90	department	department	NOUN
eurjchem-193	1	91	,	,	PUNCT
eurjchem-193	1	92	faculty	faculty	NOUN
eurjchem-193	1	93	of	of	ADP
eurjchem-193	1	94	science	science	NOUN
eurjchem-193	1	95	,	,	PUNCT
eurjchem-193	1	96	ain	ain	PROPN
eurjchem-193	1	97	shams	shams	PROPN
eurjchem-193	1	98	university	university	PROPN
eurjchem-193	1	99	,	,	PUNCT
eurjchem-193	1	100	cairo	cairo	PROPN
eurjchem-193	1	101	,	,	PUNCT
eurjchem-193	1	102	11566	11566	NUM
eurjchem-193	1	103	,	,	PUNCT
eurjchem-193	1	104	egypt	egypt	PROPN
eurjchem-193	1	105	.	.	PUNCT
eurjchem-193	2	1	tel	tel	PROPN
eurjchem-193	2	2	.	.	PUNCT
eurjchem-193	2	3	:	:	PUNCT
eurjchem-193	3	1	+2.202.4821096	+2.202.4821096	ADJ
eurjchem-193	3	2	;	;	PUNCT
eurjchem-193	3	3	fax	fax	NOUN
eurjchem-193	3	4	:	:	PUNCT
eurjchem-193	3	5	+2.202.831836	+2.202.831836	PROPN
eurjchem-193	3	6	.	.	PUNCT
eurjchem-193	3	7	e‐mail	e‐mail	PUNCT
eurjchem-193	3	8	address	address	NOUN
eurjchem-193	3	9	:	:	PUNCT
eurjchem-193	3	10	mrefaee2000@yahoo.com	mrefaee2000@yahoo.com	X
eurjchem-193	3	11	(	(	PUNCT
eurjchem-193	3	12	m.r	m.r	PROPN
eurjchem-193	3	13	.	.	PROPN
eurjchem-193	3	14	mahmoud	mahmoud	PROPN
eurjchem-193	3	15	)	)	PUNCT
eurjchem-193	3	16	.	.	PUNCT
eurjchem-193	4	1	article	article	NOUN
eurjchem-193	4	2	information	information	PROPN
eurjchem-193	4	3	abstract	abstract	ADV
eurjchem-193	4	4	received	receive	VERB
eurjchem-193	4	5	:	:	PUNCT
eurjchem-193	4	6	02	02	NUM
eurjchem-193	4	7	july	july	PROPN
eurjchem-193	4	8	2010	2010	NUM
eurjchem-193	4	9	received	receive	VERB
eurjchem-193	4	10	in	in	ADP
eurjchem-193	4	11	revised	revise	VERB
eurjchem-193	4	12	form	form	NOUN
eurjchem-193	4	13	:	:	PUNCT
eurjchem-193	4	14	14	14	NUM
eurjchem-193	4	15	october	october	NOUN
eurjchem-193	4	16	2010	2010	NUM
eurjchem-193	4	17	accepted	accept	VERB
eurjchem-193	4	18	:	:	PUNCT
eurjchem-193	4	19	08	08	NUM
eurjchem-193	4	20	december	december	PROPN
eurjchem-193	4	21	2010	2010	NUM
eurjchem-193	4	22	online	online	NOUN
eurjchem-193	4	23	:	:	PUNCT
eurjchem-193	4	24	31	31	NUM
eurjchem-193	4	25	december	december	PROPN
eurjchem-193	4	26	2011	2011	NUM
eurjchem-193	4	27	keywords	keyword	VERB
eurjchem-193	4	28	5‐arylmethylene‐2‐imino‐4‐oxo‐2‐thiazolidine	5‐arylmethylene‐2‐imino‐4‐oxo‐2‐thiazolidine	NOUN
eurjchem-193	4	29	3	3	NUM
eurjchem-193	4	30	was	be	AUX
eurjchem-193	4	31	obtained	obtain	VERB
eurjchem-193	4	32	as	as	ADP
eurjchem-193	4	33	the	the	DET
eurjchem-193	4	34	sole	sole	ADJ
eurjchem-193	4	35	product	product	NOUN
eurjchem-193	4	36	from	from	ADP
eurjchem-193	4	37	the	the	DET
eurjchem-193	4	38	reaction	reaction	NOUN
eurjchem-193	4	39	of	of	ADP
eurjchem-193	4	40	α‐cyano‐3,4,5‐trimethoxy	α‐cyano‐3,4,5‐trimethoxy	PROPN
eurjchem-193	4	41	cinnamonitrile	cinnamonitrile	NOUN
eurjchem-193	4	42	and/or	and/or	CCONJ
eurjchem-193	4	43	ethyl‐α‐cyano‐3,4,5‐trimethoxy	ethyl‐α‐cyano‐3,4,5‐trimethoxy	PROPN
eurjchem-193	4	44	cinnamate	cinnamate	NOUN
eurjchem-193	4	45	(	(	PUNCT
eurjchem-193	4	46	1a	1a	NUM
eurjchem-193	4	47	,	,	PUNCT
eurjchem-193	4	48	b	b	NOUN
eurjchem-193	4	49	)	)	PUNCT
eurjchem-193	4	50	with	with	ADP
eurjchem-193	4	51	2‐imino‐4‐oxo‐2‐thiazolidine	2‐imino‐4‐oxo‐2‐thiazolidine	NUM
eurjchem-193	4	52	2	2	NUM
eurjchem-193	4	53	.	.	PUNCT
eurjchem-193	5	1	the	the	DET
eurjchem-193	5	2	reaction	reaction	NOUN
eurjchem-193	5	3	of	of	ADP
eurjchem-193	5	4	3	3	NUM
eurjchem-193	5	5	with	with	ADP
eurjchem-193	5	6	benzyl	benzyl	NOUN
eurjchem-193	5	7	amine	amine	NOUN
eurjchem-193	5	8	gave	give	VERB
eurjchem-193	5	9	the	the	DET
eurjchem-193	5	10	imidazolidin‐4(h)one	imidazolidin‐4(h)one	NOUN
eurjchem-193	5	11	derivative	derivative	NOUN
eurjchem-193	5	12	4	4	NUM
eurjchem-193	5	13	while	while	NOUN
eurjchem-193	5	14	with	with	SCONJ
eurjchem-193	5	15	hydrazine	hydrazine	NOUN
eurjchem-193	5	16	hydrate	hydrate	NOUN
eurjchem-193	5	17	afforded	afford	VERB
eurjchem-193	5	18	the	the	DET
eurjchem-193	5	19	dimeric	dimeric	ADJ
eurjchem-193	5	20	product	product	NOUN
eurjchem-193	5	21	5	5	NUM
eurjchem-193	5	22	.	.	PUNCT
eurjchem-193	6	1	also	also	ADV
eurjchem-193	6	2	,	,	PUNCT
eurjchem-193	6	3	reaction	reaction	NOUN
eurjchem-193	6	4	of	of	ADP
eurjchem-193	6	5	thiazolidinone	thiazolidinone	NOUN
eurjchem-193	6	6	derivative	derivative	ADJ
eurjchem-193	6	7	3	3	NUM
eurjchem-193	6	8	with	with	ADP
eurjchem-193	6	9	piperidine	piperidine	NOUN
eurjchem-193	6	10	gave	give	VERB
eurjchem-193	6	11	thiazol‐4(5h)one	thiazol‐4(5h)one	PRON
eurjchem-193	6	12	derivative	derivative	NOUN
eurjchem-193	6	13	6	6	NUM
eurjchem-193	6	14	which	which	PRON
eurjchem-193	6	15	on	on	ADP
eurjchem-193	6	16	treatment	treatment	NOUN
eurjchem-193	6	17	with	with	ADP
eurjchem-193	6	18	grignard	grignard	ADJ
eurjchem-193	6	19	reagent	reagent	NOUN
eurjchem-193	6	20	and	and	CCONJ
eurjchem-193	6	21	active	active	ADJ
eurjchem-193	6	22	methylene	methylene	NOUN
eurjchem-193	6	23	compounds	compound	NOUN
eurjchem-193	6	24	afforded	afford	VERB
eurjchem-193	6	25	thiazolidin‐4‐one	thiazolidin‐4‐one	NUM
eurjchem-193	6	26	derivatives	derivative	NOUN
eurjchem-193	6	27	7‐9	7‐9	NOUN
eurjchem-193	6	28	,	,	PUNCT
eurjchem-193	6	29	respectively	respectively	ADV
eurjchem-193	6	30	.	.	PUNCT
eurjchem-193	7	1	compound	compound	NOUN
eurjchem-193	7	2	6	6	NUM
eurjchem-193	7	3	was	be	AUX
eurjchem-193	7	4	converted	convert	VERB
eurjchem-193	7	5	to	to	ADP
eurjchem-193	7	6	the	the	DET
eurjchem-193	7	7	potassium	potassium	NOUN
eurjchem-193	7	8	salt	salt	NOUN
eurjchem-193	7	9	10	10	NUM
eurjchem-193	7	10	which	which	PRON
eurjchem-193	7	11	treated	treat	VERB
eurjchem-193	7	12	with	with	ADP
eurjchem-193	7	13	acetic	acetic	ADJ
eurjchem-193	7	14	acid	acid	NOUN
eurjchem-193	7	15	,	,	PUNCT
eurjchem-193	7	16	ethyl	ethyl	PROPN
eurjchem-193	7	17	chloroacetate	chloroacetate	NOUN
eurjchem-193	7	18	and	and	CCONJ
eurjchem-193	7	19	furoyl	furoyl	PROPN
eurjchem-193	7	20	chloride	chloride	NOUN
eurjchem-193	7	21	to	to	PART
eurjchem-193	7	22	give	give	VERB
eurjchem-193	7	23	the	the	DET
eurjchem-193	7	24	compounds	compound	NOUN
eurjchem-193	7	25	11‐13	11‐13	VERB
eurjchem-193	7	26	,	,	PUNCT
eurjchem-193	7	27	respectively	respectively	ADV
eurjchem-193	7	28	.	.	PUNCT
eurjchem-193	8	1	the	the	DET
eurjchem-193	8	2	structures	structure	NOUN
eurjchem-193	8	3	of	of	ADP
eurjchem-193	8	4	all	all	DET
eurjchem-193	8	5	new	new	ADJ
eurjchem-193	8	6	compounds	compound	NOUN
eurjchem-193	8	7	were	be	AUX
eurjchem-193	8	8	evidenced	evidence	VERB
eurjchem-193	8	9	by	by	ADP
eurjchem-193	8	10	microanalytical	microanalytical	ADJ
eurjchem-193	8	11	data	datum	NOUN
eurjchem-193	8	12	and	and	CCONJ
eurjchem-193	8	13	spectral	spectral	ADJ
eurjchem-193	8	14	data	datum	NOUN
eurjchem-193	8	15	.	.	PUNCT
eurjchem-193	9	1	iminothiazolidinone	iminothiazolidinone	NOUN
eurjchem-193	9	2	derivatives	derivative	NOUN
eurjchem-193	9	3	grignard	grignard	NOUN
eurjchem-193	9	4	reagents	reagent	NOUN
eurjchem-193	9	5	imidazolidinone	imidazolidinone	VERB
eurjchem-193	9	6	derivative	derivative	ADJ
eurjchem-193	9	7	2‐thiazolidin‐4‐one	2‐thiazolidin‐4‐one	NUM
eurjchem-193	9	8	nitrogen	nitrogen	NOUN
eurjchem-193	9	9	nucleophiles	nucleophile	NOUN
eurjchem-193	9	10	activated	activate	VERB
eurjchem-193	9	11	nitriles	nitrile	NOUN
eurjchem-193	9	12	1	1	NUM
eurjchem-193	9	13	.	.	PUNCT
eurjchem-193	9	14	introduction	introduction	NOUN
eurjchem-193	9	15	in	in	ADP
eurjchem-193	9	16	connection	connection	NOUN
eurjchem-193	9	17	with	with	ADP
eurjchem-193	9	18	our	our	PRON
eurjchem-193	9	19	program	program	NOUN
eurjchem-193	9	20	of	of	ADP
eurjchem-193	9	21	preparing	prepare	VERB
eurjchem-193	9	22	heterocyclic	heterocyclic	ADJ
eurjchem-193	9	23	compounds	compound	NOUN
eurjchem-193	9	24	which	which	PRON
eurjchem-193	9	25	might	might	AUX
eurjchem-193	9	26	have	have	VERB
eurjchem-193	9	27	potential	potential	ADJ
eurjchem-193	9	28	biological	biological	ADJ
eurjchem-193	9	29	activities	activity	NOUN
eurjchem-193	10	1	[	[	X
eurjchem-193	10	2	1‐	1‐	NUM
eurjchem-193	10	3	7	7	NUM
eurjchem-193	10	4	]	]	PUNCT
eurjchem-193	10	5	.	.	PUNCT
eurjchem-193	11	1	the	the	DET
eurjchem-193	11	2	reaction	reaction	NOUN
eurjchem-193	11	3	of	of	ADP
eurjchem-193	11	4	activated	activate	VERB
eurjchem-193	11	5	nitriles	nitrile	NOUN
eurjchem-193	11	6	with	with	ADP
eurjchem-193	11	7	2‐thiazolidine	2‐thiazolidine	ADJ
eurjchem-193	11	8	derivatives	derivative	NOUN
eurjchem-193	11	9	has	have	AUX
eurjchem-193	11	10	previously	previously	ADV
eurjchem-193	11	11	claimed	claim	VERB
eurjchem-193	11	12	to	to	PART
eurjchem-193	11	13	afford	afford	VERB
eurjchem-193	11	14	the	the	DET
eurjchem-193	11	15	thiazolopyrimidine	thiazolopyrimidine	NOUN
eurjchem-193	11	16	derivatives	derivative	NOUN
eurjchem-193	11	17	in	in	ADP
eurjchem-193	11	18	moderate	moderate	ADJ
eurjchem-193	11	19	yield	yield	NOUN
eurjchem-193	11	20	[	[	X
eurjchem-193	11	21	8,9	8,9	NUM
eurjchem-193	11	22	]	]	PUNCT
eurjchem-193	11	23	.	.	PUNCT
eurjchem-193	12	1	we	we	PRON
eurjchem-193	12	2	report	report	VERB
eurjchem-193	12	3	here	here	ADV
eurjchem-193	12	4	that	that	SCONJ
eurjchem-193	12	5	no	no	DET
eurjchem-193	12	6	thiazolopyrimidine	thiazolopyrimidine	NOUN
eurjchem-193	12	7	3	3	X
eurjchem-193	12	8	'	'	PUNCT
eurjchem-193	12	9	could	could	AUX
eurjchem-193	12	10	be	be	AUX
eurjchem-193	12	11	isolated	isolate	VERB
eurjchem-193	12	12	in	in	ADP
eurjchem-193	12	13	the	the	DET
eurjchem-193	12	14	reaction	reaction	NOUN
eurjchem-193	12	15	of	of	ADP
eurjchem-193	12	16	α‐cyano‐3,4,5‐trimethoxy	α‐cyano‐3,4,5‐trimethoxy	PROPN
eurjchem-193	12	17	cinnamonitrile	cinnamonitrile	NOUN
eurjchem-193	12	18	and/or	and/or	CCONJ
eurjchem-193	12	19	ethyl‐α‐cyano‐3,4,5‐trimethoxy	ethyl‐α‐cyano‐3,4,5‐trimethoxy	PROPN
eurjchem-193	12	20	cinnamate	cinnamate	NOUN
eurjchem-193	12	21	(	(	PUNCT
eurjchem-193	12	22	1a	1a	NUM
eurjchem-193	12	23	,	,	PUNCT
eurjchem-193	12	24	b	b	NOUN
eurjchem-193	12	25	)	)	PUNCT
eurjchem-193	12	26	with	with	ADP
eurjchem-193	12	27	2‐imino‐	2‐imino‐	NUM
eurjchem-193	12	28	4‐oxo‐2‐thiazolidine	4‐oxo‐2‐thiazolidine	NOUN
eurjchem-193	12	29	2	2	NUM
eurjchem-193	13	1	and	and	CCONJ
eurjchem-193	13	2	instead	instead	ADV
eurjchem-193	13	3	we	we	PRON
eurjchem-193	13	4	have	have	AUX
eurjchem-193	13	5	found	find	VERB
eurjchem-193	13	6	that	that	SCONJ
eurjchem-193	13	7	the	the	DET
eurjchem-193	13	8	reaction	reaction	NOUN
eurjchem-193	13	9	product	product	NOUN
eurjchem-193	13	10	in	in	ADP
eurjchem-193	13	11	all	all	DET
eurjchem-193	13	12	cases	case	NOUN
eurjchem-193	13	13	was	be	AUX
eurjchem-193	13	14	5‐arylmethylene‐2‐imino‐4‐	5‐arylmethylene‐2‐imino‐4‐	NUM
eurjchem-193	13	15	oxo‐2‐thiazolidine	oxo‐2‐thiazolidine	PROPN
eurjchem-193	13	16	3	3	NUM
eurjchem-193	13	17	.	.	NOUN
eurjchem-193	13	18	2	2	NUM
eurjchem-193	13	19	.	.	X
eurjchem-193	13	20	experimental	experimental	ADJ
eurjchem-193	13	21	all	all	DET
eurjchem-193	13	22	melting	melt	VERB
eurjchem-193	13	23	points	point	NOUN
eurjchem-193	13	24	are	be	AUX
eurjchem-193	13	25	uncorrected	uncorrecte	VERB
eurjchem-193	13	26	.	.	PUNCT
eurjchem-193	14	1	the	the	DET
eurjchem-193	14	2	infrared	infrared	ADJ
eurjchem-193	14	3	spectra	spectra	NOUN
eurjchem-193	14	4	are	be	AUX
eurjchem-193	14	5	recorded	record	VERB
eurjchem-193	14	6	on	on	ADP
eurjchem-193	14	7	ftir	ftir	PROPN
eurjchem-193	14	8	maltson	maltson	PROPN
eurjchem-193	14	9	(	(	PUNCT
eurjchem-193	14	10	infinity	infinity	NOUN
eurjchem-193	14	11	series	series	NOUN
eurjchem-193	14	12	)	)	PUNCT
eurjchem-193	14	13	spectrometers	spectrometer	NOUN
eurjchem-193	14	14	as	as	ADP
eurjchem-193	14	15	kbr	kbr	PROPN
eurjchem-193	14	16	discs	disc	NOUN
eurjchem-193	14	17	.	.	PUNCT
eurjchem-193	15	1	the	the	DET
eurjchem-193	15	2	1h	1h	NUM
eurjchem-193	15	3	nmr	nmr	NOUN
eurjchem-193	15	4	spectra	spectra	NOUN
eurjchem-193	15	5	were	be	AUX
eurjchem-193	15	6	measured	measure	VERB
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eurjchem-193	15	8	varian	varian	PROPN
eurjchem-193	15	9	gemini	gemini	PROPN
eurjchem-193	15	10	200	200	NUM
eurjchem-193	15	11	mhz	mhz	NOUN
eurjchem-193	15	12	instrument	instrument	NOUN
eurjchem-193	15	13	with	with	ADP
eurjchem-193	15	14	chemical	chemical	ADJ
eurjchem-193	15	15	shift	shift	NOUN
eurjchem-193	15	16	(	(	PUNCT
eurjchem-193	15	17			NUM
eurjchem-193	15	18	)	)	PUNCT
eurjchem-193	15	19	expressed	express	VERB
eurjchem-193	15	20	in	in	ADP
eurjchem-193	15	21	ppm	ppm	ADJ
eurjchem-193	15	22	downfield	downfield	NOUN
eurjchem-193	15	23	from	from	ADP
eurjchem-193	15	24	tms	tms	PROPN
eurjchem-193	15	25	.	.	PUNCT
eurjchem-193	16	1	mass	mass	PROPN
eurjchem-193	16	2	spectra	spectra	PROPN
eurjchem-193	16	3	were	be	AUX
eurjchem-193	16	4	recorded	record	VERB
eurjchem-193	16	5	on	on	ADP
eurjchem-193	16	6	shimaduzu	shimaduzu	PROPN
eurjchem-193	16	7	gc‐ms	gc‐ms	PROPN
eurjchem-193	16	8	,	,	PUNCT
eurjchem-193	16	9	qp	qp	ADP
eurjchem-193	16	10	1000	1000	NUM
eurjchem-193	16	11	ex	ex	X
eurjchem-193	16	12	instrument	instrument	NOUN
eurjchem-193	16	13	operating	operate	VERB
eurjchem-193	16	14	at	at	ADP
eurjchem-193	16	15	70	70	NUM
eurjchem-193	16	16	ev	ev	NOUN
eurjchem-193	16	17	.	.	PROPN
eurjchem-193	16	18	tlc	tlc	PROPN
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eurjchem-193	16	20	run	run	VERB
eurjchem-193	16	21	using	use	VERB
eurjchem-193	16	22	tlc	tlc	NOUN
eurjchem-193	16	23	aluminum	aluminum	NOUN
eurjchem-193	16	24	sheets	sheet	NOUN
eurjchem-193	16	25	silica	silica	NOUN
eurjchem-193	16	26	gel	gel	NOUN
eurjchem-193	16	27	f254	f254	PROPN
eurjchem-193	16	28	(	(	PUNCT
eurjchem-193	16	29	merck	merck	PROPN
eurjchem-193	16	30	)	)	PUNCT
eurjchem-193	16	31	.	.	PUNCT
eurjchem-193	17	1	(	(	PUNCT
eurjchem-193	17	2	z)‐2‐imino‐5‐(3,4,5‐trimethoxybenzylidene)‐thiazolidin‐4‐	z)‐2‐imino‐5‐(3,4,5‐trimethoxybenzylidene)‐thiazolidin‐4‐	NUM
eurjchem-193	17	3	one	one	NUM
eurjchem-193	17	4	(	(	PUNCT
eurjchem-193	17	5	3	3	NUM
eurjchem-193	17	6	):	):	PUNCT
eurjchem-193	17	7	a	a	DET
eurjchem-193	17	8	mixture	mixture	NOUN
eurjchem-193	17	9	of	of	ADP
eurjchem-193	17	10	iminothiazolidinone	iminothiazolidinone	NOUN
eurjchem-193	17	11	2	2	NUM
eurjchem-193	17	12	(	(	PUNCT
eurjchem-193	17	13	1.16	1.16	NUM
eurjchem-193	17	14	g	g	NOUN
eurjchem-193	17	15	,	,	PUNCT
eurjchem-193	17	16	10	10	NUM
eurjchem-193	17	17	mmole	mmole	NOUN
eurjchem-193	17	18	)	)	PUNCT
eurjchem-193	17	19	,	,	PUNCT
eurjchem-193	17	20	0.5	0.5	NUM
eurjchem-193	17	21	ml	ml	NOUN
eurjchem-193	17	22	piperidine	piperidine	NOUN
eurjchem-193	17	23	,	,	PUNCT
eurjchem-193	17	24	α‐cyano‐3,4,5‐trimethoxy	α‐cyano‐3,4,5‐trimethoxy	PROPN
eurjchem-193	17	25	cinnamonitrile	cinnamonitrile	NOUN
eurjchem-193	17	26	1a	1a	NOUN
eurjchem-193	17	27	and/or	and/or	CCONJ
eurjchem-193	17	28	ethyl‐α‐cyano‐3,4,5‐trimethoxy	ethyl‐α‐cyano‐3,4,5‐trimethoxy	PROPN
eurjchem-193	17	29	cinnamate	cinnamate	PROPN
eurjchem-193	17	30	1b	1b	NUM
eurjchem-193	17	31	(	(	PUNCT
eurjchem-193	17	32	10	10	NUM
eurjchem-193	17	33	mmole	mmole	NOUN
eurjchem-193	17	34	)	)	PUNCT
eurjchem-193	17	35	was	be	AUX
eurjchem-193	17	36	refluxed	refluxe	VERB
eurjchem-193	17	37	in	in	ADP
eurjchem-193	17	38	30	30	NUM
eurjchem-193	17	39	ml	ml	NOUN
eurjchem-193	17	40	absolute	absolute	ADJ
eurjchem-193	17	41	ethanol	ethanol	NOUN
eurjchem-193	17	42	for	for	ADP
eurjchem-193	17	43	6h	6h	NUM
eurjchem-193	17	44	.	.	PUNCT
eurjchem-193	18	1	the	the	DET
eurjchem-193	18	2	solid	solid	ADJ
eurjchem-193	18	3	product	product	NOUN
eurjchem-193	18	4	deposited	deposit	VERB
eurjchem-193	18	5	on	on	ADP
eurjchem-193	18	6	hot	hot	ADJ
eurjchem-193	18	7	was	be	AUX
eurjchem-193	18	8	filtered	filter	VERB
eurjchem-193	18	9	off	off	ADP
eurjchem-193	18	10	,	,	PUNCT
eurjchem-193	18	11	washed	wash	VERB
eurjchem-193	18	12	with	with	ADP
eurjchem-193	18	13	hot	hot	ADJ
eurjchem-193	18	14	water	water	NOUN
eurjchem-193	18	15	,	,	PUNCT
eurjchem-193	18	16	dried	dry	VERB
eurjchem-193	18	17	and	and	CCONJ
eurjchem-193	18	18	recrystallized	recrystallize	VERB
eurjchem-193	18	19	from	from	ADP
eurjchem-193	18	20	n‐butanol	n‐butanol	ADV
eurjchem-193	18	21	as	as	ADV
eurjchem-193	18	22	yellow	yellow	ADJ
eurjchem-193	18	23	crystals	crystal	NOUN
eurjchem-193	18	24	(	(	PUNCT
eurjchem-193	18	25	scheme	scheme	NOUN
eurjchem-193	18	26	1	1	NUM
eurjchem-193	18	27	)	)	PUNCT
eurjchem-193	18	28	.	.	PUNCT
eurjchem-193	19	1	yield	yield	NOUN
eurjchem-193	19	2	:	:	PUNCT
eurjchem-193	19	3	48	48	NUM
eurjchem-193	19	4	%	%	NOUN
eurjchem-193	19	5	.	.	PUNCT
eurjchem-193	20	1	m.p	m.p	PROPN
eurjchem-193	20	2	.	.	PROPN
eurjchem-193	20	3	:	:	PUNCT
eurjchem-193	21	1	263‐265	263‐265	PROPN
eurjchem-193	21	2	°	°	NUM
eurjchem-193	21	3	c	c	X
eurjchem-193	21	4	.	.	PUNCT
eurjchem-193	22	1	ft‐ir	ft‐ir	NOUN
eurjchem-193	22	2	(	(	PUNCT
eurjchem-193	22	3	kbr	kbr	PROPN
eurjchem-193	22	4	,	,	PUNCT
eurjchem-193	22	5	cm‐1	cm‐1	PROPN
eurjchem-193	22	6	):	):	PUNCT
eurjchem-193	22	7	3171	3171	NUM
eurjchem-193	22	8	ν(nh	ν(nh	NOUN
eurjchem-193	22	9	)	)	PUNCT
eurjchem-193	22	10	,	,	PUNCT
eurjchem-193	22	11	3076	3076	NUM
eurjchem-193	22	12	ν(c‐harom	ν(c‐harom	NOUN
eurjchem-193	22	13	)	)	PUNCT
eurjchem-193	22	14	,	,	PUNCT
eurjchem-193	22	15	2936	2936	NUM
eurjchem-193	22	16	,	,	PUNCT
eurjchem-193	22	17	2860	2860	NUM
eurjchem-193	22	18	ν(c‐halkyl	ν(c‐halkyl	NOUN
eurjchem-193	22	19	)	)	PUNCT
eurjchem-193	22	20	,	,	PUNCT
eurjchem-193	22	21	1678	1678	NUM
eurjchem-193	22	22	ν(co	ν(co	NOUN
eurjchem-193	22	23	)	)	PUNCT
eurjchem-193	22	24	,	,	PUNCT
eurjchem-193	22	25	1638	1638	NUM
eurjchem-193	22	26	ν(c	ν(c	NOUN
eurjchem-193	22	27	=	=	SYM
eurjchem-193	22	28	n	n	NUM
eurjchem-193	22	29	)	)	PUNCT
eurjchem-193	22	30	.	.	PUNCT
eurjchem-193	23	1	1h	1h	NUM
eurjchem-193	23	2	nmr	nmr	NOUN
eurjchem-193	23	3	(	(	PUNCT
eurjchem-193	23	4	200	200	NUM
eurjchem-193	23	5	mhz	mhz	NOUN
eurjchem-193	23	6	,	,	PUNCT
eurjchem-193	23	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-193	23	8	,	,	PUNCT
eurjchem-193	23	9	ppm	ppm	NOUN
eurjchem-193	23	10	):	):	PUNCT
eurjchem-193	23	11	9.36	9.36	NUM
eurjchem-193	23	12	(	(	PUNCT
eurjchem-193	23	13	s	s	PROPN
eurjchem-193	23	14	,	,	PUNCT
eurjchem-193	23	15	1h	1h	NUM
eurjchem-193	23	16	,	,	PUNCT
eurjchem-193	23	17	nh	nh	PROPN
eurjchem-193	23	18	,	,	PUNCT
eurjchem-193	23	19	exchangeable	exchangeable	ADJ
eurjchem-193	23	20	with	with	ADP
eurjchem-193	23	21	d2o	d2o	NOUN
eurjchem-193	23	22	)	)	PUNCT
eurjchem-193	23	23	,	,	PUNCT
eurjchem-193	23	24	8	8	NUM
eurjchem-193	23	25	(	(	PUNCT
eurjchem-193	23	26	s	s	PROPN
eurjchem-193	23	27	,	,	PUNCT
eurjchem-193	23	28	1h	1h	NUM
eurjchem-193	23	29	,	,	PUNCT
eurjchem-193	23	30	nh	nh	PROPN
eurjchem-193	23	31	,	,	PUNCT
eurjchem-193	23	32	exchangeable	exchangeable	ADJ
eurjchem-193	23	33	with	with	ADP
eurjchem-193	23	34	d2o	d2o	NOUN
eurjchem-193	23	35	)	)	PUNCT
eurjchem-193	23	36	,	,	PUNCT
eurjchem-193	23	37	7.3	7.3	NUM
eurjchem-193	23	38	(	(	PUNCT
eurjchem-193	23	39	s	s	PROPN
eurjchem-193	23	40	,	,	PUNCT
eurjchem-193	23	41	1h	1h	NUM
eurjchem-193	23	42	,	,	PUNCT
eurjchem-193	23	43	=	=	NOUN
eurjchem-193	23	44	ch	ch	NOUN
eurjchem-193	23	45	)	)	PUNCT
eurjchem-193	23	46	,	,	PUNCT
eurjchem-193	23	47	6.7	6.7	NUM
eurjchem-193	23	48	(	(	PUNCT
eurjchem-193	23	49	br.s	br.s	PROPN
eurjchem-193	23	50	,	,	PUNCT
eurjchem-193	23	51	2harom	2harom	NUM
eurjchem-193	23	52	.	.	PUNCT
eurjchem-193	23	53	)	)	PUNCT
eurjchem-193	23	54	,	,	PUNCT
eurjchem-193	23	55	3.9	3.9	NUM
eurjchem-193	23	56	(	(	PUNCT
eurjchem-193	23	57	s	s	PROPN
eurjchem-193	23	58	,	,	PUNCT
eurjchem-193	23	59	6h	6h	NUM
eurjchem-193	23	60	,	,	PUNCT
eurjchem-193	23	61	2ome	2ome	PROPN
eurjchem-193	23	62	)	)	PUNCT
eurjchem-193	23	63	,	,	PUNCT
eurjchem-193	23	64	3.85	3.85	NUM
eurjchem-193	23	65	(	(	PUNCT
eurjchem-193	23	66	s	s	PROPN
eurjchem-193	23	67	,	,	PUNCT
eurjchem-193	23	68	3h	3h	NUM
eurjchem-193	23	69	,	,	PUNCT
eurjchem-193	23	70	ome	ome	PROPN
eurjchem-193	23	71	)	)	PUNCT
eurjchem-193	23	72	.	.	PUNCT
eurjchem-193	24	1	13c	13c	NOUN
eurjchem-193	24	2	nmr	nmr	NOUN
eurjchem-193	24	3	(	(	PUNCT
eurjchem-193	24	4	200	200	NUM
eurjchem-193	24	5	mhz	mhz	NOUN
eurjchem-193	24	6	,	,	PUNCT
eurjchem-193	24	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-193	24	8	,	,	PUNCT
eurjchem-193	24	9	ppm	ppm	NOUN
eurjchem-193	24	10	):	):	PUNCT
eurjchem-193	24	11	159.3	159.3	NUM
eurjchem-193	24	12	(	(	PUNCT
eurjchem-193	24	13	c4	c4	NOUN
eurjchem-193	24	14	)	)	PUNCT
eurjchem-193	24	15	,	,	PUNCT
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eurjchem-193	24	17	(	(	PUNCT
eurjchem-193	24	18	c3	c3	PROPN
eurjchem-193	24	19	'	'	PROPN
eurjchem-193	24	20	,	,	PUNCT
eurjchem-193	24	21	c5	c5	PROPN
eurjchem-193	24	22	'	'	PUNCT
eurjchem-193	24	23	)	)	PUNCT
eurjchem-193	24	24	,	,	PUNCT
eurjchem-193	24	25	146.7	146.7	NUM
eurjchem-193	24	26	(	(	PUNCT
eurjchem-193	24	27	c2	c2	PROPN
eurjchem-193	24	28	)	)	PUNCT
eurjchem-193	24	29	,	,	PUNCT
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eurjchem-193	24	31	(	(	PUNCT
eurjchem-193	24	32	c4	c4	NOUN
eurjchem-193	24	33	'	'	PUNCT
eurjchem-193	24	34	)	)	PUNCT
eurjchem-193	24	35	,	,	PUNCT
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eurjchem-193	24	37	(	(	PUNCT
eurjchem-193	24	38	c6	c6	PROPN
eurjchem-193	24	39	)	)	PUNCT
eurjchem-193	24	40	,	,	PUNCT
eurjchem-193	24	41	128.6	128.6	NUM
eurjchem-193	24	42	(	(	PUNCT
eurjchem-193	24	43	c1	c1	PROPN
eurjchem-193	24	44	'	'	PUNCT
eurjchem-193	24	45	)	)	PUNCT
eurjchem-193	24	46	,	,	PUNCT
eurjchem-193	24	47	128.6	128.6	NUM
eurjchem-193	24	48	(	(	PUNCT
eurjchem-193	24	49	c1	c1	PROPN
eurjchem-193	24	50	'	'	PUNCT
eurjchem-193	24	51	)	)	PUNCT
eurjchem-193	24	52	,	,	PUNCT
eurjchem-193	24	53	114.2	114.2	NUM
eurjchem-193	24	54	(	(	PUNCT
eurjchem-193	24	55	c5	c5	PROPN
eurjchem-193	24	56	)	)	PUNCT
eurjchem-193	24	57	,	,	PUNCT
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eurjchem-193	24	60	c2	c2	PROPN
eurjchem-193	24	61	'	'	PUNCT
eurjchem-193	24	62	)	)	PUNCT
eurjchem-193	24	63	,	,	PUNCT
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eurjchem-193	24	65	(	(	PUNCT
eurjchem-193	24	66	c4'‐	c4'‐	NOUN
eurjchem-193	24	67	ome	ome	PROPN
eurjchem-193	24	68	)	)	PUNCT
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eurjchem-193	24	72	)	)	PUNCT
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eurjchem-193	25	2	(	(	PUNCT
eurjchem-193	25	3	ei	ei	PROPN
eurjchem-193	25	4	,	,	PUNCT
eurjchem-193	25	5	m	m	PROPN
eurjchem-193	25	6	/	/	SYM
eurjchem-193	25	7	z	z	PROPN
eurjchem-193	25	8	(	(	PUNCT
eurjchem-193	25	9	%	%	NOUN
eurjchem-193	25	10	)	)	PUNCT
eurjchem-193	25	11	):	):	PUNCT
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eurjchem-193	25	13	(	(	PUNCT
eurjchem-193	25	14	m	m	PROPN
eurjchem-193	25	15	,	,	PUNCT
eurjchem-193	25	16	75.9	75.9	NUM
eurjchem-193	25	17	)	)	PUNCT
eurjchem-193	25	18	,	,	PUNCT
eurjchem-193	25	19	224	224	NUM
eurjchem-193	25	20	(	(	PUNCT
eurjchem-193	25	21	m‐	m‐	PROPN
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eurjchem-193	25	23	,	,	PUNCT
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eurjchem-193	25	25	.	.	PUNCT
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eurjchem-193	26	2	)	)	PUNCT
eurjchem-193	26	3	,	,	PUNCT
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eurjchem-193	26	5	(	(	PUNCT
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eurjchem-193	26	7	,	,	PUNCT
eurjchem-193	26	8	100	100	NUM
eurjchem-193	26	9	)	)	PUNCT
eurjchem-193	26	10	,	,	PUNCT
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eurjchem-193	26	12	(	(	PUNCT
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eurjchem-193	26	14	)	)	PUNCT
eurjchem-193	26	15	,	,	PUNCT
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eurjchem-193	26	17	(	(	PUNCT
eurjchem-193	26	18	61.8	61.8	NUM
eurjchem-193	26	19	)	)	PUNCT
eurjchem-193	26	20	.	.	PUNCT
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eurjchem-193	27	2	.	.	PUNCT
eurjchem-193	27	3	calcd	calcd	NOUN
eurjchem-193	27	4	.	.	PUNCT
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eurjchem-193	28	2	c13h14n2o4s	c13h14n2o4s	PROPN
eurjchem-193	28	3	(	(	PUNCT
eurjchem-193	28	4	294.31	294.31	NUM
eurjchem-193	28	5	):	):	PUNCT
eurjchem-193	28	6	c	c	X
eurjchem-193	28	7	,	,	PUNCT
eurjchem-193	28	8	53.05	53.05	NUM
eurjchem-193	28	9	;	;	PUNCT
eurjchem-193	28	10	h	h	NOUN
eurjchem-193	28	11	,	,	PUNCT
eurjchem-193	28	12	4.78	4.78	NUM
eurjchem-193	28	13	;	;	PUNCT
eurjchem-193	28	14	n	n	CCONJ
eurjchem-193	28	15	,	,	PUNCT
eurjchem-193	28	16	9.51	9.51	NUM
eurjchem-193	28	17	.	.	PUNCT
eurjchem-193	28	18	found	find	VERB
eurjchem-193	28	19	:	:	PUNCT
eurjchem-193	29	1	c	c	X
eurjchem-193	29	2	,	,	PUNCT
eurjchem-193	29	3	52.83	52.83	NUM
eurjchem-193	29	4	;	;	PUNCT
eurjchem-193	29	5	h	h	NOUN
eurjchem-193	29	6	,	,	PUNCT
eurjchem-193	29	7	5.1	5.1	NUM
eurjchem-193	29	8	;	;	PUNCT
eurjchem-193	29	9	n	n	CCONJ
eurjchem-193	29	10	,	,	PUNCT
eurjchem-193	29	11	10.0	10.0	NUM
eurjchem-193	29	12	%	%	NOUN
eurjchem-193	29	13	.	.	PUNCT
eurjchem-193	30	1	(	(	PUNCT
eurjchem-193	30	2	2e	2e	NOUN
eurjchem-193	30	3	,	,	PUNCT
eurjchem-193	30	4	5z)‐1‐benzyl‐2‐benzylimino‐5‐(3,4,5‐trimethoxybenzyli‐	5z)‐1‐benzyl‐2‐benzylimino‐5‐(3,4,5‐trimethoxybenzyli‐	ADJ
eurjchem-193	30	5	dene)‐imidazolidin‐4(h)one	dene)‐imidazolidin‐4(h)one	PROPN
eurjchem-193	30	6	(	(	PUNCT
eurjchem-193	30	7	4	4	NUM
eurjchem-193	30	8	):	):	PUNCT
eurjchem-193	30	9	a	a	DET
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eurjchem-193	30	12	3	3	NUM
eurjchem-193	30	13	(	(	PUNCT
eurjchem-193	30	14	1.47	1.47	NUM
eurjchem-193	30	15	g	g	NOUN
eurjchem-193	30	16	,	,	PUNCT
eurjchem-193	30	17	5	5	NUM
eurjchem-193	30	18	mmole	mmole	NOUN
eurjchem-193	30	19	)	)	PUNCT
eurjchem-193	30	20	and	and	CCONJ
eurjchem-193	30	21	benzyl	benzyl	NOUN
eurjchem-193	30	22	amine	amine	NOUN
eurjchem-193	30	23	(	(	PUNCT
eurjchem-193	30	24	0.53	0.53	NUM
eurjchem-193	30	25	ml	ml	NOUN
eurjchem-193	30	26	,	,	PUNCT
eurjchem-193	30	27	5	5	NUM
eurjchem-193	30	28	mmole	mmole	NOUN
eurjchem-193	30	29	)	)	PUNCT
eurjchem-193	30	30	was	be	AUX
eurjchem-193	30	31	boiled	boil	VERB
eurjchem-193	30	32	in	in	ADP
eurjchem-193	30	33	ethanol	ethanol	NOUN
eurjchem-193	30	34	(	(	PUNCT
eurjchem-193	30	35	20	20	NUM
eurjchem-193	30	36	ml	ml	NOUN
eurjchem-193	30	37	)	)	PUNCT
eurjchem-193	30	38	for	for	ADP
eurjchem-193	30	39	4	4	NUM
eurjchem-193	30	40	h	h	NOUN
eurjchem-193	30	41	(	(	PUNCT
eurjchem-193	30	42	tlc	tlc	NOUN
eurjchem-193	30	43	)	)	PUNCT
eurjchem-193	30	44	.	.	PUNCT
eurjchem-193	31	1	the	the	DET
eurjchem-193	31	2	excess	excess	ADJ
eurjchem-193	31	3	solvent	solvent	NOUN
eurjchem-193	31	4	was	be	AUX
eurjchem-193	31	5	removed	remove	VERB
eurjchem-193	31	6	and	and	CCONJ
eurjchem-193	31	7	the	the	DET
eurjchem-193	31	8	crude	crude	ADJ
eurjchem-193	31	9	oil	oil	NOUN
eurjchem-193	31	10	triturated	triturate	VERB
eurjchem-193	31	11	with	with	ADP
eurjchem-193	31	12	petroleum‐ether	petroleum‐ether	NOUN
eurjchem-193	31	13	(	(	PUNCT
eurjchem-193	31	14	b.p	b.p	PROPN
eurjchem-193	31	15	.	.	PROPN
eurjchem-193	32	1	:	:	PUNCT
eurjchem-193	32	2	40‐60	40‐60	NUM
eurjchem-193	32	3	°	°	PROPN
eurjchem-193	32	4	c	c	NOUN
eurjchem-193	32	5	)	)	PUNCT
eurjchem-193	32	6	.	.	PUNCT
eurjchem-193	33	1	the	the	DET
eurjchem-193	33	2	solid	solid	ADJ
eurjchem-193	33	3	separated	separate	VERB
eurjchem-193	33	4	was	be	AUX
eurjchem-193	33	5	filtered	filter	VERB
eurjchem-193	33	6	off	off	ADP
eurjchem-193	33	7	,	,	PUNCT
eurjchem-193	33	8	dried	dry	VERB
eurjchem-193	33	9	and	and	CCONJ
eurjchem-193	33	10	then	then	ADV
eurjchem-193	33	11	recrystallized	recrystallize	VERB
eurjchem-193	33	12	from	from	ADP
eurjchem-193	33	13	light	light	ADJ
eurjchem-193	33	14	petroleum‐ether	petroleum‐ether	NOUN
eurjchem-193	33	15	(	(	PUNCT
eurjchem-193	33	16	b.p	b.p	PROPN
eurjchem-193	33	17	.	.	PROPN
eurjchem-193	33	18	:	:	PUNCT
eurjchem-193	34	1	80‐100	80‐100	PROPN
eurjchem-193	34	2	°	°	NUM
eurjchem-193	34	3	c	c	NOUN
eurjchem-193	34	4	)	)	PUNCT
eurjchem-193	34	5	to	to	PART
eurjchem-193	34	6	give	give	VERB
eurjchem-193	34	7	yellow	yellow	ADJ
eurjchem-193	34	8	crystals	crystal	NOUN
eurjchem-193	34	9	(	(	PUNCT
eurjchem-193	34	10	scheme	scheme	NOUN
eurjchem-193	34	11	3	3	NUM
eurjchem-193	34	12	)	)	PUNCT
eurjchem-193	34	13	.	.	PUNCT
eurjchem-193	35	1	yield	yield	NOUN
eurjchem-193	35	2	:	:	PUNCT
eurjchem-193	35	3	30	30	NUM
eurjchem-193	35	4	%	%	NOUN
eurjchem-193	35	5	.	.	PUNCT
eurjchem-193	36	1	m.p	m.p	PROPN
eurjchem-193	36	2	.	.	PROPN
eurjchem-193	36	3	:	:	PUNCT
eurjchem-193	37	1	120‐122	120‐122	NUM
eurjchem-193	37	2	°	°	SYM
eurjchem-193	37	3	c	c	X
eurjchem-193	37	4	.	.	PUNCT
eurjchem-193	38	1	ft‐ir	ft‐ir	NOUN
eurjchem-193	38	2	(	(	PUNCT
eurjchem-193	38	3	kbr	kbr	PROPN
eurjchem-193	38	4	,	,	PUNCT
eurjchem-193	38	5	cm‐1	cm‐1	PROPN
eurjchem-193	38	6	):	):	PUNCT
eurjchem-193	38	7	3420	3420	NUM
eurjchem-193	38	8	ν(nh	ν(nh	NOUN
eurjchem-193	38	9	)	)	PUNCT
eurjchem-193	38	10	,	,	PUNCT
eurjchem-193	38	11	3062	3062	NUM
eurjchem-193	38	12	ν(c‐harom	ν(c‐harom	NOUN
eurjchem-193	38	13	.	.	PUNCT
eurjchem-193	38	14	)	)	PUNCT
eurjchem-193	38	15	,	,	PUNCT
eurjchem-193	38	16	2938	2938	NUM
eurjchem-193	38	17	,	,	PUNCT
eurjchem-193	38	18	2840	2840	NUM
eurjchem-193	38	19	ν(c‐halkyl	ν(c‐halkyl	PROPN
eurjchem-193	38	20	.	.	PUNCT
eurjchem-193	38	21	)	)	PUNCT
eurjchem-193	38	22	,	,	PUNCT
eurjchem-193	38	23	1724	1724	NUM
eurjchem-193	38	24	ν(co	ν(co	NOUN
eurjchem-193	38	25	)	)	PUNCT
eurjchem-193	38	26	,	,	PUNCT
eurjchem-193	38	27	1652	1652	NUM
eurjchem-193	38	28	ν(c	ν(c	PROPN
eurjchem-193	38	29	=	=	SYM
eurjchem-193	38	30	n	n	CCONJ
eurjchem-193	38	31	)	)	PUNCT
eurjchem-193	38	32	,	,	PUNCT
eurjchem-193	38	33	1590	1590	NUM
eurjchem-193	38	34	ν(c	ν(c	PROPN
eurjchem-193	38	35	=	=	SYM
eurjchem-193	38	36	c	c	NOUN
eurjchem-193	38	37	)	)	PUNCT
eurjchem-193	38	38	.	.	PUNCT
eurjchem-193	39	1	1h	1h	NUM
eurjchem-193	39	2	nmr	nmr	NOUN
eurjchem-193	39	3	(	(	PUNCT
eurjchem-193	39	4	200	200	NUM
eurjchem-193	39	5	mhz	mhz	NOUN
eurjchem-193	39	6	,	,	PUNCT
eurjchem-193	39	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-193	39	8	,	,	PUNCT
eurjchem-193	39	9	ppm	ppm	NOUN
eurjchem-193	39	10	):	):	PUNCT
eurjchem-193	39	11	7.64	7.64	NUM
eurjchem-193	39	12	(	(	PUNCT
eurjchem-193	39	13	s	s	PROPN
eurjchem-193	39	14	,	,	PUNCT
eurjchem-193	39	15	1h	1h	NUM
eurjchem-193	39	16	,	,	PUNCT
eurjchem-193	39	17	nh	nh	PROPN
eurjchem-193	39	18	,	,	PUNCT
eurjchem-193	39	19	exchangeable	exchangeable	ADJ
eurjchem-193	39	20	with	with	ADP
eurjchem-193	39	21	d2o	d2o	NOUN
eurjchem-193	39	22	)	)	PUNCT
eurjchem-193	39	23	,	,	PUNCT
eurjchem-193	39	24	7.5	7.5	NUM
eurjchem-193	39	25	(	(	PUNCT
eurjchem-193	39	26	m	m	PROPN
eurjchem-193	39	27	,	,	PUNCT
eurjchem-193	39	28	10harom	10harom	NUM
eurjchem-193	39	29	.	.	PUNCT
eurjchem-193	39	30	)	)	PUNCT
eurjchem-193	39	31	,	,	PUNCT
eurjchem-193	39	32	7.1	7.1	NUM
eurjchem-193	39	33	(	(	PUNCT
eurjchem-193	39	34	s	s	PROPN
eurjchem-193	39	35	,	,	PUNCT
eurjchem-193	39	36	1h	1h	NUM
eurjchem-193	39	37	,	,	PUNCT
eurjchem-193	39	38	=	=	NOUN
eurjchem-193	39	39	ch	ch	NOUN
eurjchem-193	39	40	)	)	PUNCT
eurjchem-193	39	41	,	,	PUNCT
eurjchem-193	39	42	6.9	6.9	NUM
eurjchem-193	39	43	(	(	PUNCT
eurjchem-193	39	44	s	s	PROPN
eurjchem-193	39	45	,	,	PUNCT
eurjchem-193	39	46	2harom	2harom	NUM
eurjchem-193	39	47	.	.	PUNCT
eurjchem-193	39	48	)	)	PUNCT
eurjchem-193	39	49	,	,	PUNCT
eurjchem-193	39	50	4.6	4.6	NUM
eurjchem-193	39	51	(	(	PUNCT
eurjchem-193	39	52	br.s	br.s	PROPN
eurjchem-193	39	53	,	,	PUNCT
eurjchem-193	39	54	4h	4h	NOUN
eurjchem-193	39	55	,	,	PUNCT
eurjchem-193	39	56	‐nch2ph	‐nch2ph	NOUN
eurjchem-193	39	57	)	)	PUNCT
eurjchem-193	39	58	,	,	PUNCT
eurjchem-193	39	59	3.92	3.92	NUM
eurjchem-193	39	60	(	(	PUNCT
eurjchem-193	39	61	s	s	PROPN
eurjchem-193	39	62	,	,	PUNCT
eurjchem-193	39	63	6h	6h	NUM
eurjchem-193	39	64	,	,	PUNCT
eurjchem-193	39	65	2ome	2ome	PROPN
eurjchem-193	39	66	)	)	PUNCT
eurjchem-193	39	67	,	,	PUNCT
eurjchem-193	39	68	3.79	3.79	NUM
eurjchem-193	39	69	(	(	PUNCT
eurjchem-193	39	70	s	s	PROPN
eurjchem-193	39	71	,	,	PUNCT
eurjchem-193	39	72	3h	3h	NUM
eurjchem-193	39	73	,	,	PUNCT
eurjchem-193	39	74	ome	ome	PROPN
eurjchem-193	39	75	)	)	PUNCT
eurjchem-193	39	76	.	.	PUNCT
eurjchem-193	40	1	ms	ms	NOUN
eurjchem-193	40	2	(	(	PUNCT
eurjchem-193	40	3	ei	ei	PROPN
eurjchem-193	40	4	,	,	PUNCT
eurjchem-193	40	5	m	m	PROPN
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eurjchem-193	40	8	(	(	PUNCT
eurjchem-193	40	9	%	%	NOUN
eurjchem-193	40	10	)	)	PUNCT
eurjchem-193	40	11	):	):	PUNCT
eurjchem-193	40	12	457	457	NUM
eurjchem-193	40	13	(	(	PUNCT
eurjchem-193	40	14	m	m	PROPN
eurjchem-193	40	15	,	,	PUNCT
eurjchem-193	40	16	22.6	22.6	NUM
eurjchem-193	40	17	)	)	PUNCT
eurjchem-193	40	18	,	,	PUNCT
eurjchem-193	40	19	384	384	NUM
eurjchem-193	40	20	(	(	PUNCT
eurjchem-193	40	21	30.3	30.3	NUM
eurjchem-193	40	22	)	)	PUNCT
eurjchem-193	40	23	,	,	PUNCT
eurjchem-193	40	24	224	224	NUM
eurjchem-193	40	25	(	(	PUNCT
eurjchem-193	40	26	base	base	NOUN
eurjchem-193	40	27	,	,	PUNCT
eurjchem-193	40	28	100	100	NUM
eurjchem-193	40	29	)	)	PUNCT
eurjchem-193	40	30	,	,	PUNCT
eurjchem-193	40	31	210	210	NUM
eurjchem-193	40	32	(	(	PUNCT
eurjchem-193	40	33	57.8	57.8	NUM
eurjchem-193	40	34	)	)	PUNCT
eurjchem-193	40	35	,	,	PUNCT
eurjchem-193	40	36	91	91	NUM
eurjchem-193	40	37	(	(	PUNCT
eurjchem-193	40	38	25.3	25.3	NUM
eurjchem-193	40	39	)	)	PUNCT
eurjchem-193	40	40	.	.	PUNCT
eurjchem-193	41	1	anal	anal	PROPN
eurjchem-193	41	2	.	.	PUNCT
eurjchem-193	41	3	calcd	calcd	NOUN
eurjchem-193	41	4	.	.	PUNCT
eurjchem-193	42	1	for	for	ADP
eurjchem-193	42	2	c27h27n3o4	c27h27n3o4	PROPN
eurjchem-193	42	3	(	(	PUNCT
eurjchem-193	42	4	457.49	457.49	NUM
eurjchem-193	42	5	):	):	PUNCT
eurjchem-193	42	6	c	c	X
eurjchem-193	42	7	,	,	PUNCT
eurjchem-193	42	8	70.88	70.88	NUM
eurjchem-193	42	9	;	;	PUNCT
eurjchem-193	42	10	h	h	NOUN
eurjchem-193	42	11	,	,	PUNCT
eurjchem-193	42	12	5.94	5.94	NUM
eurjchem-193	42	13	;	;	PUNCT
eurjchem-193	42	14	n	n	CCONJ
eurjchem-193	42	15	,	,	PUNCT
eurjchem-193	42	16	9.18	9.18	NUM
eurjchem-193	42	17	.	.	PUNCT
eurjchem-193	42	18	found	find	VERB
eurjchem-193	42	19	:	:	PUNCT
eurjchem-193	43	1	c	c	X
eurjchem-193	43	2	,	,	PUNCT
eurjchem-193	43	3	70.36	70.36	NUM
eurjchem-193	43	4	;	;	PUNCT
eurjchem-193	44	1	h	h	NOUN
eurjchem-193	44	2	,	,	PUNCT
eurjchem-193	44	3	5.8	5.8	NUM
eurjchem-193	44	4	;	;	PUNCT
eurjchem-193	44	5	n	n	CCONJ
eurjchem-193	44	6	,	,	PUNCT
eurjchem-193	44	7	8.77	8.77	NUM
eurjchem-193	44	8	%	%	NOUN
eurjchem-193	44	9	.	.	PUNCT
eurjchem-193	45	1	(	(	PUNCT
eurjchem-193	45	2	5z,5'z)‐2,2'‐(hydrazin‐1,2‐diyl)bis[5‐(3,4,5‐trimethoxybenz‐	5z,5'z)‐2,2'‐(hydrazin‐1,2‐diyl)bis[5‐(3,4,5‐trimethoxybenz‐	NUM
eurjchem-193	45	3	ylidene)]‐thiazol‐4(5h	ylidene)]‐thiazol‐4(5h	NOUN
eurjchem-193	45	4	)	)	PUNCT
eurjchem-193	45	5	one	one	NUM
eurjchem-193	45	6	(	(	PUNCT
eurjchem-193	45	7	5	5	NUM
eurjchem-193	45	8	):	):	PUNCT
eurjchem-193	45	9	a	a	DET
eurjchem-193	45	10	mixture	mixture	NOUN
eurjchem-193	45	11	of	of	ADP
eurjchem-193	45	12	3	3	NUM
eurjchem-193	45	13	(	(	PUNCT
eurjchem-193	45	14	1.47	1.47	NUM
eurjchem-193	45	15	g	g	NOUN
eurjchem-193	45	16	,	,	PUNCT
eurjchem-193	45	17	5	5	NUM
eurjchem-193	45	18	mmole	mmole	NOUN
eurjchem-193	45	19	)	)	PUNCT
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eurjchem-193	45	22	hydrate	hydrate	NOUN
eurjchem-193	45	23	(	(	PUNCT
eurjchem-193	45	24	5	5	NUM
eurjchem-193	45	25	ml	ml	NOUN
eurjchem-193	45	26	,	,	PUNCT
eurjchem-193	45	27	10	10	NUM
eurjchem-193	45	28	mmole	mmole	NOUN
eurjchem-193	45	29	)	)	PUNCT
eurjchem-193	45	30	was	be	AUX
eurjchem-193	45	31	refluxed	refluxe	VERB
eurjchem-193	45	32	in	in	ADP
eurjchem-193	45	33	20	20	NUM
eurjchem-193	45	34	ml	ml	NOUN
eurjchem-193	45	35	n‐butanol	n‐butanol	PUNCT
eurjchem-193	45	36	for	for	ADP
eurjchem-193	45	37	0.5	0.5	NUM
eurjchem-193	45	38	h	h	NOUN
eurjchem-193	45	39	(	(	PUNCT
eurjchem-193	45	40	tlc	tlc	NOUN
eurjchem-193	45	41	)	)	PUNCT
eurjchem-193	45	42	.	.	PUNCT
eurjchem-193	46	1	the	the	DET
eurjchem-193	46	2	separated	separate	VERB
eurjchem-193	46	3	solid	solid	ADJ
eurjchem-193	46	4	was	be	AUX
eurjchem-193	46	5	filtered	filter	VERB
eurjchem-193	46	6	off	off	ADP
eurjchem-193	46	7	,	,	PUNCT
eurjchem-193	46	8	and	and	CCONJ
eurjchem-193	46	9	washed	wash	VERB
eurjchem-193	46	10	with	with	ADP
eurjchem-193	46	11	butanol	butanol	NOUN
eurjchem-193	46	12	and	and	CCONJ
eurjchem-193	46	13	recrystallized	recrystallize	VERB
eurjchem-193	46	14	from	from	ADP
eurjchem-193	46	15	dioxane	dioxane	NOUN
eurjchem-193	46	16	to	to	PART
eurjchem-193	46	17	give	give	VERB
eurjchem-193	46	18	yellow	yellow	ADJ
eurjchem-193	46	19	powder	powder	NOUN
eurjchem-193	46	20	(	(	PUNCT
eurjchem-193	46	21	scheme	scheme	NOUN
eurjchem-193	46	22	3	3	NUM
eurjchem-193	46	23	)	)	PUNCT
eurjchem-193	46	24	.	.	PUNCT
eurjchem-193	47	1	yield	yield	NOUN
eurjchem-193	47	2	:	:	PUNCT
eurjchem-193	47	3	30	30	NUM
eurjchem-193	47	4	%	%	NOUN
eurjchem-193	47	5	.	.	PUNCT
eurjchem-193	48	1	m.p	m.p	PROPN
eurjchem-193	48	2	.	.	PROPN
eurjchem-193	48	3	:	:	PUNCT
eurjchem-193	49	1	316‐318	316‐318	NUM
eurjchem-193	49	2	°	°	SYM
eurjchem-193	49	3	c	c	X
eurjchem-193	49	4	.	.	PUNCT
eurjchem-193	49	5	ft‐ir	ft‐ir	NOUN
eurjchem-193	49	6	(	(	PUNCT
eurjchem-193	49	7	kbr	kbr	PROPN
eurjchem-193	49	8	,	,	PUNCT
eurjchem-193	49	9	cm‐1	cm‐1	PROPN
eurjchem-193	49	10	):	):	PUNCT
eurjchem-193	49	11	3230	3230	NUM
eurjchem-193	49	12	ν(nh	ν(nh	NOUN
eurjchem-193	49	13	)	)	PUNCT
eurjchem-193	49	14	,	,	PUNCT
eurjchem-193	49	15	3060	3060	NUM
eurjchem-193	49	16	ν(c‐harom	ν(c‐harom	NOUN
eurjchem-193	49	17	.	.	PUNCT
eurjchem-193	49	18	)	)	PUNCT
eurjchem-193	49	19	,	,	PUNCT
eurjchem-193	49	20	2928	2928	NUM
eurjchem-193	49	21	,	,	PUNCT
eurjchem-193	49	22	2851	2851	NUM
eurjchem-193	49	23	ν(c‐halkyl	ν(c‐halkyl	PROPN
eurjchem-193	49	24	.	.	PUNCT
eurjchem-193	49	25	)	)	PUNCT
eurjchem-193	49	26	,	,	PUNCT
eurjchem-193	49	27	1707	1707	NUM
eurjchem-193	49	28	ν(co	ν(co	NUM
eurjchem-193	49	29	)	)	PUNCT
eurjchem-193	49	30	.	.	PUNCT
eurjchem-193	50	1	476	476	NUM
eurjchem-193	50	2	madmoud	madmoud	NOUN
eurjchem-193	50	3	et	et	PROPN
eurjchem-193	50	4	al	al	PROPN
eurjchem-193	50	5	.	.	PUNCT
eurjchem-193	50	6	/	/	SYM
eurjchem-193	50	7	european	european	PROPN
eurjchem-193	50	8	journal	journal	PROPN
eurjchem-193	50	9	of	of	ADP
eurjchem-193	50	10	chemistry	chemistry	NOUN
eurjchem-193	50	11	2	2	NUM
eurjchem-193	50	12	(	(	PUNCT
eurjchem-193	50	13	4	4	NUM
eurjchem-193	50	14	)	)	PUNCT
eurjchem-193	50	15	(	(	PUNCT
eurjchem-193	50	16	2011	2011	NUM
eurjchem-193	50	17	)	)	PUNCT
eurjchem-193	50	18	475‐479	475‐479	NUM
eurjchem-193	50	19	meo	meo	PROPN
eurjchem-193	50	20	meo	meo	PROPN
eurjchem-193	50	21	ome	ome	PROPN
eurjchem-193	50	22	h	h	NOUN
eurjchem-193	50	23	cn	cn	PROPN
eurjchem-193	50	24	z	z	PROPN
eurjchem-193	50	25	(	(	PUNCT
eurjchem-193	50	26	1	1	NUM
eurjchem-193	50	27	)	)	PUNCT
eurjchem-193	50	28	z	z	NOUN
eurjchem-193	50	29	=	=	SYM
eurjchem-193	50	30	cn	cn	PROPN
eurjchem-193	50	31	,	,	PUNCT
eurjchem-193	50	32	co2c2h5	co2c2h5	PROPN
eurjchem-193	51	1	+	+	CCONJ
eurjchem-193	51	2	nh	nh	PROPN
eurjchem-193	51	3	s	s	PART
eurjchem-193	51	4	hn	hn	PROPN
eurjchem-193	51	5	o	o	X
eurjchem-193	51	6	(	(	PUNCT
eurjchem-193	51	7	2	2	NUM
eurjchem-193	51	8	)	)	PUNCT
eurjchem-193	51	9	etoh	etoh	PROPN
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eurjchem-193	51	11	.	.	PUNCT
eurjchem-193	52	1	nh	nh	PROPN
eurjchem-193	52	2	s	s	PART
eurjchem-193	53	1	hn	hn	NOUN
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eurjchem-193	53	3	h	h	NOUN
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eurjchem-193	53	7	(	(	PUNCT
eurjchem-193	53	8	3	3	NUM
eurjchem-193	53	9	)	)	PUNCT
eurjchem-193	53	10	n	n	CCONJ
eurjchem-193	53	11	n	n	PROPN
eurjchem-193	53	12	s	s	PART
eurjchem-193	53	13	o	o	X
eurjchem-193	53	14	h	h	NOUN
eurjchem-193	53	15	arh	arh	PROPN
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eurjchem-193	53	17	h	h	PROPN
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eurjchem-193	53	19	z	z	PROPN
eurjchem-193	53	20	(	(	PUNCT
eurjchem-193	53	21	3	3	NUM
eurjchem-193	53	22	'	'	CCONJ
eurjchem-193	53	23	)	)	PUNCT
eurjchem-193	53	24	scheme	scheme	NOUN
eurjchem-193	53	25	1	1	NUM
eurjchem-193	53	26	scheme	scheme	NOUN
eurjchem-193	53	27	2	2	NUM
eurjchem-193	53	28	1h	1h	NUM
eurjchem-193	53	29	nmr	nmr	NOUN
eurjchem-193	53	30	(	(	PUNCT
eurjchem-193	53	31	200	200	NUM
eurjchem-193	53	32	mhz	mhz	NOUN
eurjchem-193	53	33	,	,	PUNCT
eurjchem-193	53	34	dmso‐d6	dmso‐d6	NOUN
eurjchem-193	53	35	,	,	PUNCT
eurjchem-193	53	36	ppm	ppm	NOUN
eurjchem-193	53	37	):	):	PUNCT
eurjchem-193	53	38	7.4	7.4	NUM
eurjchem-193	53	39	(	(	PUNCT
eurjchem-193	53	40	s	s	PROPN
eurjchem-193	53	41	,	,	PUNCT
eurjchem-193	53	42	2h	2h	NUM
eurjchem-193	53	43	)	)	PUNCT
eurjchem-193	53	44	,	,	PUNCT
eurjchem-193	53	45	6.9	6.9	NUM
eurjchem-193	53	46	(	(	PUNCT
eurjchem-193	53	47	m	m	PROPN
eurjchem-193	53	48	,	,	PUNCT
eurjchem-193	53	49	4harom	4harom	PROPN
eurjchem-193	53	50	.	.	PUNCT
eurjchem-193	53	51	)	)	PUNCT
eurjchem-193	53	52	,	,	PUNCT
eurjchem-193	53	53	3.92	3.92	NUM
eurjchem-193	53	54	(	(	PUNCT
eurjchem-193	53	55	s	s	PROPN
eurjchem-193	53	56	,	,	PUNCT
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eurjchem-193	53	58	,	,	PUNCT
eurjchem-193	53	59	4ome	4ome	PROPN
eurjchem-193	53	60	)	)	PUNCT
eurjchem-193	53	61	,	,	PUNCT
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eurjchem-193	53	63	(	(	PUNCT
eurjchem-193	53	64	s	s	PROPN
eurjchem-193	53	65	,	,	PUNCT
eurjchem-193	53	66	6h	6h	NUM
eurjchem-193	53	67	,	,	PUNCT
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eurjchem-193	53	70	,	,	PUNCT
eurjchem-193	53	71	3.1	3.1	NUM
eurjchem-193	53	72	(	(	PUNCT
eurjchem-193	53	73	br.s	br.s	PROPN
eurjchem-193	53	74	,	,	PUNCT
eurjchem-193	53	75	2h	2h	NUM
eurjchem-193	53	76	,	,	PUNCT
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eurjchem-193	53	78	,	,	PUNCT
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eurjchem-193	53	83	.	.	PUNCT
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eurjchem-193	54	4	,	,	PUNCT
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eurjchem-193	54	7	z	z	PROPN
eurjchem-193	54	8	(	(	PUNCT
eurjchem-193	54	9	%	%	NOUN
eurjchem-193	54	10	)	)	PUNCT
eurjchem-193	54	11	):	):	PUNCT
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eurjchem-193	54	13	(	(	PUNCT
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eurjchem-193	54	15	,	,	PUNCT
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eurjchem-193	54	17	)	)	PUNCT
eurjchem-193	54	18	,	,	PUNCT
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eurjchem-193	54	20	(	(	PUNCT
eurjchem-193	54	21	16.2	16.2	NUM
eurjchem-193	54	22	)	)	PUNCT
eurjchem-193	54	23	,	,	PUNCT
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eurjchem-193	54	25	(	(	PUNCT
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eurjchem-193	54	27	)	)	PUNCT
eurjchem-193	54	28	,	,	PUNCT
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eurjchem-193	54	30	(	(	PUNCT
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eurjchem-193	54	32	,	,	PUNCT
eurjchem-193	54	33	100	100	NUM
eurjchem-193	54	34	)	)	PUNCT
eurjchem-193	54	35	,	,	PUNCT
eurjchem-193	54	36	209	209	NUM
eurjchem-193	54	37	(	(	PUNCT
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eurjchem-193	54	39	,	,	PUNCT
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eurjchem-193	54	41	)	)	PUNCT
eurjchem-193	54	42	,	,	PUNCT
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eurjchem-193	54	44	(	(	PUNCT
eurjchem-193	54	45	30.1	30.1	NUM
eurjchem-193	54	46	)	)	PUNCT
eurjchem-193	54	47	.	.	PUNCT
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eurjchem-193	55	4	.	.	PUNCT
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eurjchem-193	56	3	(	(	PUNCT
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eurjchem-193	56	5	):	):	PUNCT
eurjchem-193	56	6	c	c	X
eurjchem-193	56	7	,	,	PUNCT
eurjchem-193	56	8	53.23	53.23	NUM
eurjchem-193	56	9	;	;	PUNCT
eurjchem-193	56	10	h	h	NOUN
eurjchem-193	56	11	,	,	PUNCT
eurjchem-193	56	12	4.46	4.46	NUM
eurjchem-193	56	13	;	;	PUNCT
eurjchem-193	56	14	n	n	CCONJ
eurjchem-193	56	15	,	,	PUNCT
eurjchem-193	56	16	9.55	9.55	NUM
eurjchem-193	56	17	.	.	PUNCT
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eurjchem-193	58	1	c	c	X
eurjchem-193	58	2	,	,	PUNCT
eurjchem-193	58	3	53.42	53.42	NUM
eurjchem-193	58	4	;	;	PUNCT
eurjchem-193	59	1	h	h	NOUN
eurjchem-193	59	2	,	,	PUNCT
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eurjchem-193	59	4	;	;	PUNCT
eurjchem-193	59	5	n	n	CCONJ
eurjchem-193	59	6	,	,	PUNCT
eurjchem-193	59	7	9.16	9.16	NUM
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eurjchem-193	59	9	.	.	PUNCT
eurjchem-193	60	1	(	(	PUNCT
eurjchem-193	60	2	z)‐2‐(piperidin‐1‐yl)‐5‐(3,4,5‐trimethoxybenzylidene)‐	z)‐2‐(piperidin‐1‐yl)‐5‐(3,4,5‐trimethoxybenzylidene)‐	PROPN
eurjchem-193	60	3	thiazol‐4(5h	thiazol‐4(5h	NOUN
eurjchem-193	60	4	)	)	PUNCT
eurjchem-193	60	5	one	one	NUM
eurjchem-193	60	6	(	(	PUNCT
eurjchem-193	60	7	6	6	NUM
eurjchem-193	60	8	):	):	PUNCT
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eurjchem-193	60	13	(	(	PUNCT
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eurjchem-193	60	16	,	,	PUNCT
eurjchem-193	60	17	5	5	NUM
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eurjchem-193	60	19	)	)	PUNCT
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eurjchem-193	60	21	0.5	0.5	NUM
eurjchem-193	60	22	ml	ml	NOUN
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eurjchem-193	60	26	refluxed	refluxe	VERB
eurjchem-193	60	27	in	in	ADP
eurjchem-193	60	28	20	20	NUM
eurjchem-193	60	29	ml	ml	NOUN
eurjchem-193	60	30	ethanol	ethanol	NOUN
eurjchem-193	60	31	for	for	ADP
eurjchem-193	60	32	3h	3h	NUM
eurjchem-193	60	33	.	.	PUNCT
eurjchem-193	61	1	the	the	DET
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eurjchem-193	61	6	,	,	PUNCT
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eurjchem-193	61	8	to	to	ADP
eurjchem-193	61	9	cool	cool	VERB
eurjchem-193	61	10	,	,	PUNCT
eurjchem-193	61	11	acidified	acidify	VERB
eurjchem-193	61	12	with	with	ADP
eurjchem-193	61	13	cold	cold	ADJ
eurjchem-193	61	14	dilute	dilute	NOUN
eurjchem-193	61	15	hydrochloric	hydrochloric	ADJ
eurjchem-193	61	16	acid	acid	NOUN
eurjchem-193	61	17	.	.	PUNCT
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eurjchem-193	62	2	solid	solid	ADJ
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eurjchem-193	62	7	,	,	PUNCT
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eurjchem-193	62	9	with	with	ADP
eurjchem-193	62	10	water	water	NOUN
eurjchem-193	62	11	,	,	PUNCT
eurjchem-193	62	12	dried	dry	VERB
eurjchem-193	62	13	and	and	CCONJ
eurjchem-193	62	14	then	then	ADV
eurjchem-193	62	15	recrystallized	recrystallize	VERB
eurjchem-193	62	16	from	from	ADP
eurjchem-193	62	17	benzene	benzene	NOUN
eurjchem-193	62	18	as	as	ADP
eurjchem-193	62	19	yellow	yellow	ADJ
eurjchem-193	62	20	crystals	crystal	NOUN
eurjchem-193	62	21	(	(	PUNCT
eurjchem-193	62	22	scheme	scheme	NOUN
eurjchem-193	62	23	3	3	NUM
eurjchem-193	62	24	)	)	PUNCT
eurjchem-193	62	25	.	.	PUNCT
eurjchem-193	63	1	yield	yield	NOUN
eurjchem-193	63	2	:	:	PUNCT
eurjchem-193	63	3	45	45	NUM
eurjchem-193	63	4	%	%	NOUN
eurjchem-193	63	5	.	.	PUNCT
eurjchem-193	64	1	m.p	m.p	PROPN
eurjchem-193	64	2	.	.	PROPN
eurjchem-193	64	3	:	:	PUNCT
eurjchem-193	65	1	156‐158	156‐158	NUM
eurjchem-193	65	2	°	°	NUM
eurjchem-193	65	3	c	c	X
eurjchem-193	65	4	.	.	PUNCT
eurjchem-193	66	1	ft‐ir	ft‐ir	NOUN
eurjchem-193	66	2	(	(	PUNCT
eurjchem-193	66	3	kbr	kbr	PROPN
eurjchem-193	66	4	,	,	PUNCT
eurjchem-193	66	5	cm‐1	cm‐1	PROPN
eurjchem-193	66	6	):	):	PUNCT
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eurjchem-193	66	8	ν(c‐harom	ν(c‐harom	NOUN
eurjchem-193	66	9	.	.	PROPN
eurjchem-193	66	10	)	)	PUNCT
eurjchem-193	66	11	,	,	PUNCT
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eurjchem-193	66	13	,	,	PUNCT
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eurjchem-193	66	15	ν(c‐	ν(c‐	PROPN
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eurjchem-193	66	17	.	.	PUNCT
eurjchem-193	66	18	)	)	PUNCT
eurjchem-193	66	19	,	,	PUNCT
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eurjchem-193	66	21	ν(co	ν(co	NUM
eurjchem-193	66	22	)	)	PUNCT
eurjchem-193	66	23	.	.	PUNCT
eurjchem-193	67	1	1h	1h	NUM
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eurjchem-193	67	3	(	(	PUNCT
eurjchem-193	67	4	200	200	NUM
eurjchem-193	67	5	mhz	mhz	NOUN
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eurjchem-193	67	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-193	67	8	,	,	PUNCT
eurjchem-193	67	9	ppm	ppm	NOUN
eurjchem-193	67	10	):	):	PUNCT
eurjchem-193	67	11	7.7	7.7	NUM
eurjchem-193	67	12	(	(	PUNCT
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eurjchem-193	67	16	,	,	PUNCT
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eurjchem-193	67	18	ch	ch	NOUN
eurjchem-193	67	19	)	)	PUNCT
eurjchem-193	67	20	,	,	PUNCT
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eurjchem-193	67	23	s	s	PROPN
eurjchem-193	67	24	,	,	PUNCT
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eurjchem-193	67	28	,	,	PUNCT
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eurjchem-193	67	30	(	(	PUNCT
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eurjchem-193	67	34	,	,	PUNCT
eurjchem-193	67	35	2ome	2ome	PROPN
eurjchem-193	67	36	)	)	PUNCT
eurjchem-193	67	37	,	,	PUNCT
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eurjchem-193	67	39	(	(	PUNCT
eurjchem-193	67	40	s	s	PROPN
eurjchem-193	67	41	,	,	PUNCT
eurjchem-193	67	42	3h	3h	NUM
eurjchem-193	67	43	,	,	PUNCT
eurjchem-193	67	44	ome	ome	PROPN
eurjchem-193	67	45	)	)	PUNCT
eurjchem-193	67	46	,	,	PUNCT
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eurjchem-193	67	50	,	,	PUNCT
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eurjchem-193	67	55	.	.	PUNCT
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eurjchem-193	68	3	(	(	PUNCT
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eurjchem-193	68	5	mhz	mhz	NOUN
eurjchem-193	68	6	,	,	PUNCT
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eurjchem-193	68	8	,	,	PUNCT
eurjchem-193	68	9	ppm	ppm	NOUN
eurjchem-193	68	10	):	):	PUNCT
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eurjchem-193	68	12	(	(	PUNCT
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eurjchem-193	68	14	)	)	PUNCT
eurjchem-193	68	15	,	,	PUNCT
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eurjchem-193	68	17	(	(	PUNCT
eurjchem-193	68	18	c2	c2	PROPN
eurjchem-193	68	19	)	)	PUNCT
eurjchem-193	68	20	,	,	PUNCT
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eurjchem-193	68	22	(	(	PUNCT
eurjchem-193	68	23	c3	c3	PROPN
eurjchem-193	68	24	'	'	PROPN
eurjchem-193	68	25	,	,	PUNCT
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eurjchem-193	68	27	'	'	PUNCT
eurjchem-193	68	28	)	)	PUNCT
eurjchem-193	68	29	,	,	PUNCT
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eurjchem-193	68	31	(	(	PUNCT
eurjchem-193	68	32	c6	c6	PROPN
eurjchem-193	68	33	)	)	PUNCT
eurjchem-193	68	34	,	,	PUNCT
eurjchem-193	68	35	140.1	140.1	NUM
eurjchem-193	68	36	(	(	PUNCT
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eurjchem-193	68	38	'	'	PUNCT
eurjchem-193	68	39	)	)	PUNCT
eurjchem-193	68	40	,	,	PUNCT
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eurjchem-193	68	42	(	(	PUNCT
eurjchem-193	68	43	c5	c5	PROPN
eurjchem-193	68	44	)	)	PUNCT
eurjchem-193	68	45	,	,	PUNCT
eurjchem-193	68	46	128.1	128.1	NUM
eurjchem-193	68	47	(	(	PUNCT
eurjchem-193	68	48	c1	c1	PROPN
eurjchem-193	68	49	'	'	PUNCT
eurjchem-193	68	50	)	)	PUNCT
eurjchem-193	68	51	,	,	PUNCT
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eurjchem-193	68	53	(	(	PUNCT
eurjchem-193	68	54	c2	c2	PROPN
eurjchem-193	68	55	'	'	PUNCT
eurjchem-193	68	56	,	,	PUNCT
eurjchem-193	68	57	c6	c6	PROPN
eurjchem-193	68	58	'	'	PUNCT
eurjchem-193	68	59	)	)	PUNCT
eurjchem-193	68	60	,	,	PUNCT
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eurjchem-193	68	62	,	,	PUNCT
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eurjchem-193	68	64	,	,	PUNCT
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eurjchem-193	68	68	)	)	PUNCT
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eurjchem-193	68	73	,	,	PUNCT
eurjchem-193	68	74	24	24	NUM
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eurjchem-193	68	76	piperidyl	piperidyl	ADJ
eurjchem-193	68	77	carbons	carbon	NOUN
eurjchem-193	68	78	)	)	PUNCT
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eurjchem-193	69	8	(	(	PUNCT
eurjchem-193	69	9	%	%	NOUN
eurjchem-193	69	10	)	)	PUNCT
eurjchem-193	69	11	):	):	PUNCT
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eurjchem-193	69	13	(	(	PUNCT
eurjchem-193	69	14	m	m	PROPN
eurjchem-193	69	15	,	,	PUNCT
eurjchem-193	69	16	1.5	1.5	NUM
eurjchem-193	69	17	)	)	PUNCT
eurjchem-193	69	18	,	,	PUNCT
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eurjchem-193	69	20	(	(	PUNCT
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eurjchem-193	69	22	,	,	PUNCT
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eurjchem-193	69	24	)	)	PUNCT
eurjchem-193	69	25	,	,	PUNCT
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eurjchem-193	69	27	(	(	PUNCT
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eurjchem-193	69	29	,	,	PUNCT
eurjchem-193	69	30	100	100	NUM
eurjchem-193	69	31	)	)	PUNCT
eurjchem-193	69	32	,	,	PUNCT
eurjchem-193	69	33	330	330	NUM
eurjchem-193	69	34	(	(	PUNCT
eurjchem-193	69	35	m‐s	m‐s	PROPN
eurjchem-193	69	36	,	,	PUNCT
eurjchem-193	69	37	98.2	98.2	NUM
eurjchem-193	69	38	)	)	PUNCT
eurjchem-193	69	39	,	,	PUNCT
eurjchem-193	69	40	111	111	NUM
eurjchem-193	69	41	(	(	PUNCT
eurjchem-193	69	42	52.9	52.9	NUM
eurjchem-193	69	43	)	)	PUNCT
eurjchem-193	69	44	.	.	PUNCT
eurjchem-193	70	1	anal	anal	PROPN
eurjchem-193	70	2	.	.	PUNCT
eurjchem-193	70	3	calcd	calcd	NOUN
eurjchem-193	70	4	.	.	PUNCT
eurjchem-193	71	1	for	for	ADP
eurjchem-193	71	2	c18h22n2o4s	c18h22n2o4s	NUM
eurjchem-193	71	3	(	(	PUNCT
eurjchem-193	71	4	362.41	362.41	NUM
eurjchem-193	71	5	):	):	PUNCT
eurjchem-193	71	6	c	c	X
eurjchem-193	71	7	,	,	PUNCT
eurjchem-193	71	8	59.65	59.65	NUM
eurjchem-193	71	9	;	;	PUNCT
eurjchem-193	71	10	h	h	NOUN
eurjchem-193	71	11	,	,	PUNCT
eurjchem-193	71	12	6.11	6.11	NUM
eurjchem-193	71	13	;	;	PUNCT
eurjchem-193	71	14	n	n	CCONJ
eurjchem-193	71	15	,	,	PUNCT
eurjchem-193	71	16	7.72	7.72	NUM
eurjchem-193	71	17	.	.	PUNCT
eurjchem-193	71	18	found	find	VERB
eurjchem-193	71	19	:	:	PUNCT
eurjchem-193	72	1	c	c	X
eurjchem-193	72	2	,	,	PUNCT
eurjchem-193	72	3	60.03	60.03	NUM
eurjchem-193	72	4	;	;	PUNCT
eurjchem-193	72	5	h	h	NOUN
eurjchem-193	72	6	,	,	PUNCT
eurjchem-193	72	7	5.87	5.87	NUM
eurjchem-193	72	8	;	;	PUNCT
eurjchem-193	72	9	n	n	CCONJ
eurjchem-193	72	10	,	,	PUNCT
eurjchem-193	72	11	7.26	7.26	NUM
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eurjchem-193	72	13	.	.	PUNCT
eurjchem-193	73	1	a	a	DET
eurjchem-193	73	2	solution	solution	NOUN
eurjchem-193	73	3	of	of	ADP
eurjchem-193	73	4	phenyl	phenyl	NOUN
eurjchem-193	73	5	magnesium	magnesium	NOUN
eurjchem-193	73	6	bromide	bromide	NOUN
eurjchem-193	73	7	or	or	CCONJ
eurjchem-193	73	8	cyclohexyl	cyclohexyl	PROPN
eurjchem-193	73	9	magnesium	magnesium	NOUN
eurjchem-193	73	10	bromide	bromide	NOUN
eurjchem-193	73	11	(	(	PUNCT
eurjchem-193	73	12	15	15	NUM
eurjchem-193	73	13	mmole	mmole	NOUN
eurjchem-193	73	14	)	)	PUNCT
eurjchem-193	73	15	in	in	ADP
eurjchem-193	73	16	anhydrous	anhydrous	ADJ
eurjchem-193	73	17	ether	ether	NOUN
eurjchem-193	73	18	(	(	PUNCT
eurjchem-193	73	19	100	100	NUM
eurjchem-193	73	20	ml	ml	NOUN
eurjchem-193	73	21	)	)	PUNCT
eurjchem-193	73	22	was	be	AUX
eurjchem-193	73	23	added	add	VERB
eurjchem-193	73	24	dropwise	dropwise	NOUN
eurjchem-193	73	25	while	while	SCONJ
eurjchem-193	73	26	shaking	shake	VERB
eurjchem-193	73	27	to	to	ADP
eurjchem-193	73	28	a	a	DET
eurjchem-193	73	29	warm	warm	ADJ
eurjchem-193	73	30	solution	solution	NOUN
eurjchem-193	73	31	of	of	ADP
eurjchem-193	73	32	4‐oxo‐2‐thiazoline	4‐oxo‐2‐thiazoline	NUM
eurjchem-193	73	33	6	6	NUM
eurjchem-193	73	34	(	(	PUNCT
eurjchem-193	73	35	1.81	1.81	NUM
eurjchem-193	73	36	g	g	NOUN
eurjchem-193	73	37	,	,	PUNCT
eurjchem-193	73	38	5	5	NUM
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eurjchem-193	73	40	)	)	PUNCT
eurjchem-193	73	41	in	in	ADP
eurjchem-193	73	42	anhydrous	anhydrous	ADJ
eurjchem-193	73	43	benzene	benzene	NOUN
eurjchem-193	73	44	(	(	PUNCT
eurjchem-193	73	45	100	100	NUM
eurjchem-193	73	46	ml	ml	NOUN
eurjchem-193	73	47	)	)	PUNCT
eurjchem-193	73	48	.	.	PUNCT
eurjchem-193	74	1	the	the	DET
eurjchem-193	74	2	whole	whole	ADJ
eurjchem-193	74	3	mixture	mixture	NOUN
eurjchem-193	74	4	warmed	warm	VERB
eurjchem-193	74	5	over	over	ADP
eurjchem-193	74	6	a	a	DET
eurjchem-193	74	7	water‐bath	water‐bath	NOUN
eurjchem-193	74	8	for	for	ADP
eurjchem-193	74	9	10	10	NUM
eurjchem-193	74	10	hours	hour	NOUN
eurjchem-193	74	11	and	and	CCONJ
eurjchem-193	74	12	left	leave	VERB
eurjchem-193	74	13	standing	stand	VERB
eurjchem-193	74	14	at	at	ADP
eurjchem-193	74	15	room	room	NOUN
eurjchem-193	74	16	temperature	temperature	NOUN
eurjchem-193	74	17	for	for	ADP
eurjchem-193	74	18	24	24	NUM
eurjchem-193	74	19	hours	hour	NOUN
eurjchem-193	74	20	.	.	PUNCT
eurjchem-193	75	1	the	the	DET
eurjchem-193	75	2	grignard	grignard	ADJ
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eurjchem-193	75	5	decomposed	decompose	VERB
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eurjchem-193	75	7	a	a	DET
eurjchem-193	75	8	saturated	saturate	VERB
eurjchem-193	75	9	solution	solution	NOUN
eurjchem-193	75	10	of	of	ADP
eurjchem-193	75	11	ammonium	ammonium	NOUN
eurjchem-193	75	12	chloride	chloride	NOUN
eurjchem-193	75	13	(	(	PUNCT
eurjchem-193	75	14	200	200	NUM
eurjchem-193	75	15	ml	ml	NOUN
eurjchem-193	75	16	)	)	PUNCT
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eurjchem-193	75	18	extracted	extract	VERB
eurjchem-193	75	19	with	with	ADP
eurjchem-193	75	20	ether	ether	NOUN
eurjchem-193	75	21	(	(	PUNCT
eurjchem-193	75	22	200	200	NUM
eurjchem-193	75	23	ml	ml	NOUN
eurjchem-193	75	24	)	)	PUNCT
eurjchem-193	75	25	.	.	PUNCT
eurjchem-193	76	1	the	the	DET
eurjchem-193	76	2	combined	combine	VERB
eurjchem-193	76	3	ether‐benzene	ether‐benzene	NOUN
eurjchem-193	76	4	extract	extract	NOUN
eurjchem-193	76	5	was	be	AUX
eurjchem-193	76	6	washed	wash	VERB
eurjchem-193	76	7	thoroughly	thoroughly	ADV
eurjchem-193	76	8	with	with	ADP
eurjchem-193	76	9	water	water	NOUN
eurjchem-193	76	10	,	,	PUNCT
eurjchem-193	76	11	dried	dry	VERB
eurjchem-193	76	12	over	over	ADP
eurjchem-193	76	13	anhydrous	anhydrous	ADJ
eurjchem-193	76	14	sodium	sodium	NOUN
eurjchem-193	76	15	sulphate	sulphate	NOUN
eurjchem-193	76	16	and	and	CCONJ
eurjchem-193	76	17	evaporated	evaporate	VERB
eurjchem-193	76	18	.	.	PUNCT
eurjchem-193	77	1	the	the	DET
eurjchem-193	77	2	viscous	viscous	ADJ
eurjchem-193	77	3	oil	oil	NOUN
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eurjchem-193	77	6	was	be	AUX
eurjchem-193	77	7	triturated	triturate	VERB
eurjchem-193	77	8	several	several	ADJ
eurjchem-193	77	9	times	time	NOUN
eurjchem-193	77	10	with	with	ADP
eurjchem-193	77	11	light	light	NOUN
eurjchem-193	77	12	petroleum‐ether	petroleum‐ether	NOUN
eurjchem-193	77	13	(	(	PUNCT
eurjchem-193	77	14	b.p	b.p	PROPN
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eurjchem-193	77	16	:	:	PUNCT
eurjchem-193	77	17	40‐60	40‐60	X
eurjchem-193	78	1	°	°	PROPN
eurjchem-193	78	2	c	c	NOUN
eurjchem-193	78	3	)	)	PUNCT
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eurjchem-193	78	5	the	the	DET
eurjchem-193	78	6	remain	remain	ADJ
eurjchem-193	78	7	insoluble	insoluble	ADJ
eurjchem-193	78	8	fraction	fraction	NOUN
eurjchem-193	78	9	was	be	AUX
eurjchem-193	78	10	dissolved	dissolve	VERB
eurjchem-193	78	11	in	in	ADP
eurjchem-193	78	12	a	a	DET
eurjchem-193	78	13	suitable	suitable	ADJ
eurjchem-193	78	14	solvent	solvent	NOUN
eurjchem-193	78	15	to	to	PART
eurjchem-193	78	16	give	give	VERB
eurjchem-193	78	17	7	7	NUM
eurjchem-193	78	18	and	and	CCONJ
eurjchem-193	78	19	8	8	NUM
eurjchem-193	78	20	,	,	PUNCT
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eurjchem-193	78	22	.	.	PUNCT
eurjchem-193	79	1	2‐phenyl‐5‐[phenyl(3,4,5‐trimethoxyphenyl)methyl]‐2‐	2‐phenyl‐5‐[phenyl(3,4,5‐trimethoxyphenyl)methyl]‐2‐	NUM
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eurjchem-193	79	4	(	(	PUNCT
eurjchem-193	79	5	7	7	NUM
eurjchem-193	79	6	):	):	PUNCT
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eurjchem-193	79	9	light	light	ADJ
eurjchem-193	79	10	petroleum‐ether	petroleum‐ether	NOUN
eurjchem-193	79	11	(	(	PUNCT
eurjchem-193	79	12	b.p	b.p	PROPN
eurjchem-193	79	13	.	.	PROPN
eurjchem-193	79	14	:	:	PUNCT
eurjchem-193	80	1	80‐100	80‐100	PROPN
eurjchem-193	80	2	°	°	NUM
eurjchem-193	80	3	c	c	NOUN
eurjchem-193	80	4	)	)	PUNCT
eurjchem-193	80	5	as	as	ADP
eurjchem-193	80	6	pink	pink	ADJ
eurjchem-193	80	7	crystals	crystal	NOUN
eurjchem-193	80	8	(	(	PUNCT
eurjchem-193	80	9	scheme	scheme	NOUN
eurjchem-193	80	10	3	3	NUM
eurjchem-193	80	11	)	)	PUNCT
eurjchem-193	80	12	.	.	PUNCT
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eurjchem-193	81	2	:	:	PUNCT
eurjchem-193	81	3	36	36	NUM
eurjchem-193	81	4	%	%	NOUN
eurjchem-193	81	5	.	.	PUNCT
eurjchem-193	82	1	m.p.:160‐162	m.p.:160‐162	PROPN
eurjchem-193	83	1	°	°	ADP
eurjchem-193	83	2	c	c	X
eurjchem-193	83	3	.	.	PUNCT
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eurjchem-193	84	2	(	(	PUNCT
eurjchem-193	84	3	kbr	kbr	PROPN
eurjchem-193	84	4	,	,	PUNCT
eurjchem-193	84	5	cm‐1	cm‐1	PROPN
eurjchem-193	84	6	):	):	PUNCT
eurjchem-193	84	7	3404	3404	NUM
eurjchem-193	84	8	ν(br	ν(br	PROPN
eurjchem-193	84	9	.	.	PUNCT
eurjchem-193	84	10	nh	nh	PROPN
eurjchem-193	84	11	)	)	PUNCT
eurjchem-193	84	12	,	,	PUNCT
eurjchem-193	84	13	3072	3072	NUM
eurjchem-193	84	14	ν(c‐harom	ν(c‐harom	NOUN
eurjchem-193	84	15	.	.	PUNCT
eurjchem-193	84	16	)	)	PUNCT
eurjchem-193	84	17	,	,	PUNCT
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eurjchem-193	84	19	,	,	PUNCT
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eurjchem-193	84	22	.	.	PUNCT
eurjchem-193	84	23	)	)	PUNCT
eurjchem-193	84	24	,	,	PUNCT
eurjchem-193	84	25	1667	1667	NUM
eurjchem-193	84	26	ν(co	ν(co	NUM
eurjchem-193	84	27	)	)	PUNCT
eurjchem-193	84	28	.	.	PUNCT
eurjchem-193	85	1	1h	1h	NUM
eurjchem-193	85	2	nmr	nmr	NOUN
eurjchem-193	85	3	(	(	PUNCT
eurjchem-193	85	4	200	200	NUM
eurjchem-193	85	5	mhz	mhz	NOUN
eurjchem-193	85	6	,	,	PUNCT
eurjchem-193	85	7	cdcl3	cdcl3	NOUN
eurjchem-193	85	8	,	,	PUNCT
eurjchem-193	85	9	ppm	ppm	NUM
eurjchem-193	85	10	):	):	PUNCT
eurjchem-193	85	11	8.0	8.0	NUM
eurjchem-193	85	12	(	(	PUNCT
eurjchem-193	85	13	s	s	PROPN
eurjchem-193	85	14	,	,	PUNCT
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eurjchem-193	85	16	,	,	PUNCT
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eurjchem-193	85	23	,	,	PUNCT
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eurjchem-193	85	25	(	(	PUNCT
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eurjchem-193	85	27	,	,	PUNCT
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eurjchem-193	85	30	)	)	PUNCT
eurjchem-193	85	31	,	,	PUNCT
eurjchem-193	85	32	5.1	5.1	NUM
eurjchem-193	85	33	(	(	PUNCT
eurjchem-193	85	34	d	d	NOUN
eurjchem-193	85	35	,	,	PUNCT
eurjchem-193	85	36	j	j	PROPN
eurjchem-193	85	37	=	=	SYM
eurjchem-193	85	38	5.8	5.8	NUM
eurjchem-193	85	39	hz	hz	NOUN
eurjchem-193	85	40	,	,	PUNCT
eurjchem-193	85	41	1hbenzylic	1hbenzylic	NUM
eurjchem-193	85	42	)	)	PUNCT
eurjchem-193	85	43	,	,	PUNCT
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eurjchem-193	85	45	(	(	PUNCT
eurjchem-193	85	46	d	d	PROPN
eurjchem-193	85	47	,	,	PUNCT
eurjchem-193	85	48	1h	1h	NUM
eurjchem-193	85	49	,	,	PUNCT
eurjchem-193	85	50	j	j	PROPN
eurjchem-193	85	51	=	=	SYM
eurjchem-193	85	52	5.6	5.6	NUM
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eurjchem-193	85	54	,	,	PUNCT
eurjchem-193	85	55	c5‐h	c5‐h	PROPN
eurjchem-193	85	56	)	)	PUNCT
eurjchem-193	85	57	,	,	PUNCT
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eurjchem-193	85	59	(	(	PUNCT
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eurjchem-193	85	63	,	,	PUNCT
eurjchem-193	85	64	3ome	3ome	NUM
eurjchem-193	85	65	)	)	PUNCT
eurjchem-193	85	66	,	,	PUNCT
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eurjchem-193	85	75	)	)	PUNCT
eurjchem-193	85	76	.	.	PUNCT
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eurjchem-193	86	2	(	(	PUNCT
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eurjchem-193	86	4	,	,	PUNCT
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eurjchem-193	86	8	(	(	PUNCT
eurjchem-193	86	9	%	%	NOUN
eurjchem-193	86	10	)	)	PUNCT
eurjchem-193	86	11	):	):	PUNCT
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eurjchem-193	86	13	(	(	PUNCT
eurjchem-193	86	14	m	m	PROPN
eurjchem-193	86	15	,	,	PUNCT
eurjchem-193	86	16	3.7	3.7	NUM
eurjchem-193	86	17	)	)	PUNCT
eurjchem-193	86	18	,	,	PUNCT
eurjchem-193	86	19	502	502	NUM
eurjchem-193	86	20	(	(	PUNCT
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eurjchem-193	86	22	,	,	PUNCT
eurjchem-193	86	23	3.4	3.4	NUM
eurjchem-193	86	24	)	)	PUNCT
eurjchem-193	86	25	,	,	PUNCT
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eurjchem-193	86	27	(	(	PUNCT
eurjchem-193	86	28	4.4	4.4	NUM
eurjchem-193	86	29	)	)	PUNCT
eurjchem-193	86	30	,	,	PUNCT
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eurjchem-193	86	32	(	(	PUNCT
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eurjchem-193	86	34	,	,	PUNCT
eurjchem-193	86	35	100	100	NUM
eurjchem-193	86	36	)	)	PUNCT
eurjchem-193	86	37	,	,	PUNCT
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eurjchem-193	86	39	(	(	PUNCT
eurjchem-193	86	40	base‐me	base‐me	ADP
eurjchem-193	86	41	,	,	PUNCT
eurjchem-193	86	42	37.9	37.9	NUM
eurjchem-193	86	43	)	)	PUNCT
eurjchem-193	86	44	,	,	PUNCT
eurjchem-193	86	45	166	166	NUM
eurjchem-193	86	46	(	(	PUNCT
eurjchem-193	86	47	base‐3ch2o	base‐3ch2o	NOUN
eurjchem-193	86	48	,	,	PUNCT
eurjchem-193	86	49	20.2	20.2	NUM
eurjchem-193	86	50	)	)	PUNCT
eurjchem-193	86	51	.	.	PUNCT
eurjchem-193	87	1	anal	anal	PROPN
eurjchem-193	87	2	.	.	PUNCT
eurjchem-193	87	3	calcd	calcd	NOUN
eurjchem-193	87	4	.	.	PUNCT
eurjchem-193	88	1	for	for	SCONJ
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eurjchem-193	88	3	(	(	PUNCT
eurjchem-193	88	4	518.63	518.63	NUM
eurjchem-193	88	5	):	):	PUNCT
eurjchem-193	88	6	c	c	X
eurjchem-193	88	7	,	,	PUNCT
eurjchem-193	88	8	69.47	69.47	NUM
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eurjchem-193	88	10	h	h	NOUN
eurjchem-193	88	11	,	,	PUNCT
eurjchem-193	88	12	6.59	6.59	NUM
eurjchem-193	88	13	;	;	PUNCT
eurjchem-193	88	14	n	n	CCONJ
eurjchem-193	88	15	,	,	PUNCT
eurjchem-193	88	16	5.40	5.40	NUM
eurjchem-193	88	17	.	.	PUNCT
eurjchem-193	88	18	found	find	VERB
eurjchem-193	88	19	:	:	PUNCT
eurjchem-193	89	1	c	c	X
eurjchem-193	89	2	,	,	PUNCT
eurjchem-193	89	3	70.09	70.09	NUM
eurjchem-193	89	4	;	;	PUNCT
eurjchem-193	89	5	h	h	NOUN
eurjchem-193	89	6	,	,	PUNCT
eurjchem-193	89	7	6.42	6.42	NUM
eurjchem-193	89	8	;	;	PUNCT
eurjchem-193	89	9	n	n	CCONJ
eurjchem-193	89	10	,	,	PUNCT
eurjchem-193	89	11	5.00	5.00	NUM
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eurjchem-193	89	13	.	.	PUNCT
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eurjchem-193	90	2	z)‐2‐cyclohexyl‐2‐(piperidin‐1‐yl)‐5‐(3,4,5‐trimethoxy‐	z)‐2‐cyclohexyl‐2‐(piperidin‐1‐yl)‐5‐(3,4,5‐trimethoxy‐	PROPN
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eurjchem-193	90	4	(	(	PUNCT
eurjchem-193	90	5	8)	8)	NUM
eurjchem-193	90	6	:	:	PUNCT
eurjchem-193	90	7	recrystallized	recrystallize	VERB
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eurjchem-193	90	9	light	light	ADJ
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eurjchem-193	90	11	(	(	PUNCT
eurjchem-193	90	12	b.p	b.p	PROPN
eurjchem-193	90	13	.	.	PROPN
eurjchem-193	90	14	:	:	PUNCT
eurjchem-193	91	1	80‐100	80‐100	PROPN
eurjchem-193	91	2	°	°	NUM
eurjchem-193	91	3	c	c	NOUN
eurjchem-193	91	4	)	)	PUNCT
eurjchem-193	91	5	as	as	ADP
eurjchem-193	91	6	white	white	ADJ
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eurjchem-193	91	8	(	(	PUNCT
eurjchem-193	91	9	scheme	scheme	NOUN
eurjchem-193	91	10	3	3	NUM
eurjchem-193	91	11	)	)	PUNCT
eurjchem-193	91	12	.	.	PUNCT
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eurjchem-193	92	2	et	et	PROPN
eurjchem-193	92	3	al	al	PROPN
eurjchem-193	92	4	.	.	PUNCT
eurjchem-193	92	5	/	/	SYM
eurjchem-193	92	6	european	european	PROPN
eurjchem-193	92	7	journal	journal	PROPN
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eurjchem-193	92	9	chemistry	chemistry	NOUN
eurjchem-193	92	10	2	2	NUM
eurjchem-193	92	11	(	(	PUNCT
eurjchem-193	92	12	4	4	NUM
eurjchem-193	92	13	)	)	PUNCT
eurjchem-193	92	14	(	(	PUNCT
eurjchem-193	92	15	2011	2011	NUM
eurjchem-193	92	16	)	)	PUNCT
eurjchem-193	92	17	475‐479	475‐479	NUM
eurjchem-193	92	18	477	477	NUM
eurjchem-193	93	1	nh	nh	NOUN
eurjchem-193	93	2	s	s	VERB
eurjchem-193	93	3	hn	hn	PROPN
eurjchem-193	93	4	o	o	X
eurjchem-193	93	5	har	har	X
eurjchem-193	93	6	(	(	PUNCT
eurjchem-193	93	7	3	3	NUM
eurjchem-193	93	8	)	)	PUNCT
eurjchem-193	93	9	ph	ph	ADJ
eurjchem-193	93	10	nh2	nh2	PROPN
eurjchem-193	93	11	nh	nh	PROPN
eurjchem-193	93	12	n	n	CCONJ
eurjchem-193	93	13	n	n	ADV
eurjchem-193	93	14	o	o	X
eurjchem-193	93	15	har	har	X
eurjchem-193	93	16	ph	ph	NOUN
eurjchem-193	93	17	ph	ph	NOUN
eurjchem-193	93	18	(	(	PUNCT
eurjchem-193	93	19	4	4	NUM
eurjchem-193	93	20	)	)	PUNCT
eurjchem-193	93	21	n2h4.h2o	n2h4.h2o	NOUN
eurjchem-193	93	22	etoh	etoh	ADJ
eurjchem-193	93	23	n	n	NOUN
eurjchem-193	93	24	s	s	PART
eurjchem-193	93	25	n	n	PRON
eurjchem-193	93	26	o	o	X
eurjchem-193	93	27	har	har	X
eurjchem-193	93	28	n	n	CCONJ
eurjchem-193	93	29	n	n	NOUN
eurjchem-193	93	30	s	s	NOUN
eurjchem-193	93	31	arh	arh	ADJ
eurjchem-193	93	32	o	o	NOUN
eurjchem-193	93	33	hh	hh	PROPN
eurjchem-193	93	34	(	(	PUNCT
eurjchem-193	93	35	5	5	NUM
eurjchem-193	93	36	)	)	PUNCT
eurjchem-193	93	37	nh	nh	NOUN
eurjchem-193	93	38	etoh	etoh	PROPN
eurjchem-193	93	39	n	n	PROPN
eurjchem-193	93	40	s	s	PART
eurjchem-193	93	41	n	n	PRON
eurjchem-193	93	42	o	o	X
eurjchem-193	93	43	har	har	X
eurjchem-193	93	44	(	(	PUNCT
eurjchem-193	93	45	6	6	NUM
eurjchem-193	93	46	)	)	PUNCT
eurjchem-193	93	47	phmgbr	phmgbr	PROPN
eurjchem-193	93	48	nh	nh	PROPN
eurjchem-193	93	49	s	s	PART
eurjchem-193	93	50	n	n	PRON
eurjchem-193	93	51	o	o	X
eurjchem-193	93	52	har	har	X
eurjchem-193	93	53	(	(	PUNCT
eurjchem-193	93	54	7	7	NUM
eurjchem-193	93	55	)	)	PUNCT
eurjchem-193	93	56	ph	ph	ADJ
eurjchem-193	93	57	ph	ph	NOUN
eurjchem-193	93	58	mgbr	mgbr	PROPN
eurjchem-193	93	59	nh	nh	PROPN
eurjchem-193	93	60	s	s	PART
eurjchem-193	93	61	n	n	PRON
eurjchem-193	93	62	o	o	X
eurjchem-193	93	63	har	har	X
eurjchem-193	93	64	(	(	PUNCT
eurjchem-193	93	65	8)	8)	NUM
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eurjchem-193	93	70	n	n	PRON
eurjchem-193	93	71	o	o	X
eurjchem-193	93	72	har	har	X
eurjchem-193	93	73	(	(	PUNCT
eurjchem-193	93	74	9	9	X
eurjchem-193	93	75	)	)	PUNCT
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eurjchem-193	93	77	koh	koh	PROPN
eurjchem-193	93	78	/	/	SYM
eurjchem-193	93	79	etoh	etoh	PROPN
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eurjchem-193	93	81	s	s	PART
eurjchem-193	93	82	o	o	X
eurjchem-193	93	83	har	har	X
eurjchem-193	93	84	o	o	X
eurjchem-193	93	85	(	(	PUNCT
eurjchem-193	93	86	10	10	NUM
eurjchem-193	93	87	)	)	PUNCT
eurjchem-193	93	88	acoh	acoh	PROPN
eurjchem-193	93	89	nh	nh	PROPN
eurjchem-193	93	90	s	s	PART
eurjchem-193	93	91	o	o	X
eurjchem-193	93	92	har	har	X
eurjchem-193	93	93	o	o	X
eurjchem-193	93	94	(	(	PUNCT
eurjchem-193	93	95	11	11	NUM
eurjchem-193	93	96	)	)	PUNCT
eurjchem-193	93	97	cl	cl	NOUN
eurjchem-193	93	98	co2c2h5	co2c2h5	PROPN
eurjchem-193	93	99	n	n	PROPN
eurjchem-193	93	100	s	s	PART
eurjchem-193	93	101	o	o	X
eurjchem-193	93	102	har	har	X
eurjchem-193	93	103	o	o	X
eurjchem-193	93	104	(	(	PUNCT
eurjchem-193	93	105	12	12	NUM
eurjchem-193	93	106	)	)	PUNCT
eurjchem-193	93	107	co2c2h5	co2c2h5	PROPN
eurjchem-193	94	1	o	o	NOUN
eurjchem-193	94	2	o	o	X
eurjchem-193	94	3	cl	cl	NOUN
eurjchem-193	94	4	pyridine	pyridine	NOUN
eurjchem-193	95	1	n	n	PROPN
eurjchem-193	95	2	s	s	PART
eurjchem-193	95	3	o	o	X
eurjchem-193	95	4	har	har	X
eurjchem-193	95	5	o	o	X
eurjchem-193	95	6	(	(	PUNCT
eurjchem-193	95	7	13	13	NUM
eurjchem-193	95	8	)	)	PUNCT
eurjchem-193	96	1	o	o	NOUN
eurjchem-193	97	1	o	o	INTJ
eurjchem-193	97	2	cl	cl	NOUN
eurjchem-193	97	3	o	o	NOUN
eurjchem-193	97	4	o	o	X
eurjchem-193	97	5	scheme	scheme	NOUN
eurjchem-193	97	6	3	3	NUM
eurjchem-193	97	7	yield	yield	NOUN
eurjchem-193	97	8	:	:	PUNCT
eurjchem-193	97	9	22	22	NUM
eurjchem-193	97	10	%	%	NOUN
eurjchem-193	97	11	.	.	PUNCT
eurjchem-193	98	1	m.p	m.p	PROPN
eurjchem-193	98	2	.	.	PROPN
eurjchem-193	98	3	:	:	PUNCT
eurjchem-193	99	1	176‐178	176‐178	NUM
eurjchem-193	99	2	°	°	NUM
eurjchem-193	99	3	c	c	X
eurjchem-193	99	4	.	.	PUNCT
eurjchem-193	100	1	ft‐ir	ft‐ir	NOUN
eurjchem-193	100	2	(	(	PUNCT
eurjchem-193	100	3	kbr	kbr	PROPN
eurjchem-193	100	4	,	,	PUNCT
eurjchem-193	100	5	cm‐1	cm‐1	PROPN
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eurjchem-193	100	7	3420	3420	NUM
eurjchem-193	100	8	ν(nh	ν(nh	NOUN
eurjchem-193	100	9	)	)	PUNCT
eurjchem-193	100	10	,	,	PUNCT
eurjchem-193	100	11	3064	3064	NUM
eurjchem-193	100	12	ν(c‐harom	ν(c‐harom	NOUN
eurjchem-193	100	13	.	.	PUNCT
eurjchem-193	100	14	)	)	PUNCT
eurjchem-193	100	15	,	,	PUNCT
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eurjchem-193	100	18	.	.	PUNCT
eurjchem-193	100	19	)	)	PUNCT
eurjchem-193	100	20	,	,	PUNCT
eurjchem-193	100	21	1688	1688	NUM
eurjchem-193	100	22	ν(co	ν(co	NOUN
eurjchem-193	100	23	)	)	PUNCT
eurjchem-193	100	24	.	.	PUNCT
eurjchem-193	101	1	1h	1h	NUM
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eurjchem-193	101	3	(	(	PUNCT
eurjchem-193	101	4	200	200	NUM
eurjchem-193	101	5	mhz	mhz	NOUN
eurjchem-193	101	6	,	,	PUNCT
eurjchem-193	101	7	cdcl3	cdcl3	NOUN
eurjchem-193	101	8	,	,	PUNCT
eurjchem-193	101	9	ppm	ppm	NUM
eurjchem-193	101	10	):	):	PUNCT
eurjchem-193	101	11	7.8	7.8	NUM
eurjchem-193	101	12	(	(	PUNCT
eurjchem-193	101	13	br.s	br.s	PROPN
eurjchem-193	101	14	,	,	PUNCT
eurjchem-193	101	15	1h	1h	NUM
eurjchem-193	101	16	,	,	PUNCT
eurjchem-193	101	17	nh	nh	PROPN
eurjchem-193	101	18	,	,	PUNCT
eurjchem-193	101	19	exchangeable	exchangeable	ADJ
eurjchem-193	101	20	with	with	ADP
eurjchem-193	101	21	d2o	d2o	NOUN
eurjchem-193	101	22	)	)	PUNCT
eurjchem-193	101	23	,	,	PUNCT
eurjchem-193	101	24	7.2	7.2	NUM
eurjchem-193	101	25	(	(	PUNCT
eurjchem-193	101	26	s	s	PROPN
eurjchem-193	101	27	,	,	PUNCT
eurjchem-193	101	28	1h	1h	NUM
eurjchem-193	101	29	,	,	PUNCT
eurjchem-193	101	30	=	=	NOUN
eurjchem-193	101	31	ch	ch	NOUN
eurjchem-193	101	32	)	)	PUNCT
eurjchem-193	101	33	,	,	PUNCT
eurjchem-193	101	34	6.9	6.9	NUM
eurjchem-193	101	35	(	(	PUNCT
eurjchem-193	101	36	s	s	PROPN
eurjchem-193	101	37	,	,	PUNCT
eurjchem-193	101	38	2harom	2harom	NUM
eurjchem-193	101	39	.	.	PUNCT
eurjchem-193	101	40	)	)	PUNCT
eurjchem-193	101	41	,	,	PUNCT
eurjchem-193	101	42	3.89	3.89	NUM
eurjchem-193	101	43	(	(	PUNCT
eurjchem-193	101	44	s	s	PROPN
eurjchem-193	101	45	,	,	PUNCT
eurjchem-193	101	46	9h	9h	NUM
eurjchem-193	101	47	,	,	PUNCT
eurjchem-193	101	48	3ome	3ome	NUM
eurjchem-193	101	49	)	)	PUNCT
eurjchem-193	101	50	,	,	PUNCT
eurjchem-193	101	51	2.1‐1.6	2.1‐1.6	NUM
eurjchem-193	101	52	(	(	PUNCT
eurjchem-193	101	53	two	two	NUM
eurjchem-193	101	54	m	m	PROPN
eurjchem-193	101	55	,	,	PUNCT
eurjchem-193	101	56	10h	10h	NUM
eurjchem-193	101	57	,	,	PUNCT
eurjchem-193	101	58	c5h10	c5h10	NOUN
eurjchem-193	101	59	)	)	PUNCT
eurjchem-193	101	60	,	,	PUNCT
eurjchem-193	101	61	1.49‐1.08	1.49‐1.08	NUM
eurjchem-193	101	62	(	(	PUNCT
eurjchem-193	101	63	m	m	PROPN
eurjchem-193	101	64	,	,	PUNCT
eurjchem-193	101	65	11h	11h	NUM
eurjchem-193	101	66	,	,	PUNCT
eurjchem-193	101	67	c6h11	c6h11	NOUN
eurjchem-193	101	68	)	)	PUNCT
eurjchem-193	101	69	.	.	PUNCT
eurjchem-193	102	1	ms	ms	NOUN
eurjchem-193	102	2	(	(	PUNCT
eurjchem-193	102	3	ei	ei	PROPN
eurjchem-193	102	4	,	,	PUNCT
eurjchem-193	102	5	m	m	PROPN
eurjchem-193	102	6	/	/	SYM
eurjchem-193	102	7	z	z	PROPN
eurjchem-193	102	8	(	(	PUNCT
eurjchem-193	102	9	%	%	NOUN
eurjchem-193	102	10	)	)	PUNCT
eurjchem-193	102	11	):	):	PUNCT
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eurjchem-193	102	13	(	(	PUNCT
eurjchem-193	102	14	m	m	PROPN
eurjchem-193	102	15	,	,	PUNCT
eurjchem-193	102	16	22.7	22.7	NUM
eurjchem-193	102	17	)	)	PUNCT
eurjchem-193	102	18	,	,	PUNCT
eurjchem-193	102	19	432	432	NUM
eurjchem-193	102	20	(	(	PUNCT
eurjchem-193	102	21	m‐me	m‐me	NOUN
eurjchem-193	102	22	,	,	PUNCT
eurjchem-193	102	23	31.9	31.9	NUM
eurjchem-193	102	24	)	)	PUNCT
eurjchem-193	102	25	,	,	PUNCT
eurjchem-193	102	26	349	349	NUM
eurjchem-193	102	27	(	(	PUNCT
eurjchem-193	102	28	27.7	27.7	NUM
eurjchem-193	102	29	)	)	PUNCT
eurjchem-193	102	30	,	,	PUNCT
eurjchem-193	102	31	249	249	NUM
eurjchem-193	102	32	(	(	PUNCT
eurjchem-193	102	33	12.8	12.8	NUM
eurjchem-193	102	34	)	)	PUNCT
eurjchem-193	102	35	,	,	PUNCT
eurjchem-193	102	36	184	184	NUM
eurjchem-193	102	37	(	(	PUNCT
eurjchem-193	102	38	base	base	NOUN
eurjchem-193	102	39	,	,	PUNCT
eurjchem-193	102	40	100	100	NUM
eurjchem-193	102	41	)	)	PUNCT
eurjchem-193	102	42	.	.	PUNCT
eurjchem-193	103	1	anal	anal	PROPN
eurjchem-193	103	2	.	.	PUNCT
eurjchem-193	103	3	calcd	calcd	NOUN
eurjchem-193	103	4	.	.	PUNCT
eurjchem-193	104	1	for	for	ADP
eurjchem-193	104	2	c24h34n2o4s	c24h34n2o4s	PROPN
eurjchem-193	104	3	(	(	PUNCT
eurjchem-193	104	4	446.61	446.61	NUM
eurjchem-193	104	5	):	):	PUNCT
eurjchem-193	104	6	c	c	X
eurjchem-193	104	7	,	,	PUNCT
eurjchem-193	104	8	64.54	64.54	NUM
eurjchem-193	104	9	;	;	PUNCT
eurjchem-193	104	10	h	h	NOUN
eurjchem-193	104	11	,	,	PUNCT
eurjchem-193	104	12	7.66	7.66	NUM
eurjchem-193	104	13	;	;	PUNCT
eurjchem-193	104	14	n	n	CCONJ
eurjchem-193	104	15	,	,	PUNCT
eurjchem-193	104	16	6.27	6.27	NUM
eurjchem-193	104	17	.	.	PUNCT
eurjchem-193	104	18	found	find	VERB
eurjchem-193	104	19	:	:	PUNCT
eurjchem-193	105	1	c	c	X
eurjchem-193	105	2	,	,	PUNCT
eurjchem-193	105	3	64.56	64.56	NUM
eurjchem-193	105	4	;	;	PUNCT
eurjchem-193	105	5	h	h	X
eurjchem-193	105	6	,	,	PUNCT
eurjchem-193	105	7	7.43	7.43	NUM
eurjchem-193	105	8	;	;	PUNCT
eurjchem-193	105	9	n	n	CCONJ
eurjchem-193	105	10	,	,	PUNCT
eurjchem-193	105	11	5.91	5.91	NUM
eurjchem-193	105	12	%	%	NOUN
eurjchem-193	105	13	.	.	PUNCT
eurjchem-193	106	1	(	(	PUNCT
eurjchem-193	106	2	z)‐2‐[4‐oxo‐2‐(piperidin‐1‐yl)‐5‐(3,4,5‐trimethoxybenzyli‐	z)‐2‐[4‐oxo‐2‐(piperidin‐1‐yl)‐5‐(3,4,5‐trimethoxybenzyli‐	PROPN
eurjchem-193	106	3	dene)‐thiazolidin‐2‐yl	dene)‐thiazolidin‐2‐yl	PROPN
eurjchem-193	106	4	]	]	X
eurjchem-193	106	5	malonic	malonic	ADJ
eurjchem-193	106	6	acid	acid	NOUN
eurjchem-193	106	7	(	(	PUNCT
eurjchem-193	106	8	9	9	NUM
eurjchem-193	106	9	):	):	PUNCT
eurjchem-193	106	10	to	to	ADP
eurjchem-193	106	11	a	a	DET
eurjchem-193	106	12	stirred	stir	VERB
eurjchem-193	106	13	mixture	mixture	NOUN
eurjchem-193	106	14	of	of	ADP
eurjchem-193	106	15	6	6	NUM
eurjchem-193	106	16	(	(	PUNCT
eurjchem-193	106	17	1.81	1.81	NUM
eurjchem-193	106	18	g	g	NOUN
eurjchem-193	106	19	,	,	PUNCT
eurjchem-193	106	20	5	5	NUM
eurjchem-193	106	21	mmole	mmole	NOUN
eurjchem-193	106	22	)	)	PUNCT
eurjchem-193	106	23	,	,	PUNCT
eurjchem-193	106	24	ethylcyanoacetate	ethylcyanoacetate	NOUN
eurjchem-193	106	25	(	(	PUNCT
eurjchem-193	106	26	0.56	0.56	NUM
eurjchem-193	106	27	g	g	NOUN
eurjchem-193	106	28	,	,	PUNCT
eurjchem-193	106	29	5	5	NUM
eurjchem-193	106	30	mmole	mmole	NOUN
eurjchem-193	106	31	)	)	PUNCT
eurjchem-193	106	32	and	and	CCONJ
eurjchem-193	106	33	20	20	NUM
eurjchem-193	106	34	ml	ml	NOUN
eurjchem-193	106	35	dry	dry	ADJ
eurjchem-193	106	36	benzene	benzene	NOUN
eurjchem-193	106	37	,	,	PUNCT
eurjchem-193	106	38	sodium	sodium	NOUN
eurjchem-193	106	39	hydride	hydride	NOUN
eurjchem-193	106	40	(	(	PUNCT
eurjchem-193	106	41	0.24	0.24	NUM
eurjchem-193	106	42	g	g	NOUN
eurjchem-193	106	43	,	,	PUNCT
eurjchem-193	106	44	10	10	NUM
eurjchem-193	106	45	mmole	mmole	NOUN
eurjchem-193	106	46	)	)	PUNCT
eurjchem-193	106	47	was	be	AUX
eurjchem-193	106	48	added	add	VERB
eurjchem-193	106	49	portion	portion	NOUN
eurjchem-193	106	50	wise	wise	ADJ
eurjchem-193	106	51	and	and	CCONJ
eurjchem-193	106	52	the	the	DET
eurjchem-193	106	53	whole	whole	ADJ
eurjchem-193	106	54	mixture	mixture	NOUN
eurjchem-193	106	55	was	be	AUX
eurjchem-193	106	56	refluxed	refluxe	VERB
eurjchem-193	106	57	for	for	ADP
eurjchem-193	106	58	3	3	NUM
eurjchem-193	106	59	hrs	hrs	NOUN
eurjchem-193	106	60	until	until	ADP
eurjchem-193	106	61	no	no	DET
eurjchem-193	106	62	more	more	ADJ
eurjchem-193	106	63	substrate	substrate	NOUN
eurjchem-193	106	64	(	(	PUNCT
eurjchem-193	106	65	tlc	tlc	NOUN
eurjchem-193	106	66	)	)	PUNCT
eurjchem-193	106	67	.	.	PUNCT
eurjchem-193	107	1	the	the	DET
eurjchem-193	107	2	excess	excess	ADJ
eurjchem-193	107	3	solvent	solvent	NOUN
eurjchem-193	107	4	was	be	AUX
eurjchem-193	107	5	evaporated	evaporate	VERB
eurjchem-193	107	6	.	.	PUNCT
eurjchem-193	108	1	the	the	DET
eurjchem-193	108	2	reaction	reaction	NOUN
eurjchem-193	108	3	mixture	mixture	NOUN
eurjchem-193	108	4	was	be	AUX
eurjchem-193	108	5	treated	treat	VERB
eurjchem-193	108	6	with	with	ADP
eurjchem-193	108	7	cold	cold	ADJ
eurjchem-193	108	8	dilute	dilute	NOUN
eurjchem-193	108	9	hydrochloric	hydrochloric	ADJ
eurjchem-193	108	10	acid	acid	NOUN
eurjchem-193	108	11	.	.	PUNCT
eurjchem-193	109	1	the	the	DET
eurjchem-193	109	2	separated	separate	VERB
eurjchem-193	109	3	solid	solid	ADJ
eurjchem-193	109	4	was	be	AUX
eurjchem-193	109	5	collected	collect	VERB
eurjchem-193	109	6	by	by	ADP
eurjchem-193	109	7	suction	suction	NOUN
eurjchem-193	109	8	,	,	PUNCT
eurjchem-193	109	9	washed	wash	VERB
eurjchem-193	109	10	with	with	ADP
eurjchem-193	109	11	water	water	NOUN
eurjchem-193	109	12	,	,	PUNCT
eurjchem-193	109	13	dried	dry	VERB
eurjchem-193	109	14	and	and	CCONJ
eurjchem-193	109	15	then	then	ADV
eurjchem-193	109	16	recrystallized	recrystallize	VERB
eurjchem-193	109	17	from	from	ADP
eurjchem-193	109	18	benzene	benzene	NOUN
eurjchem-193	109	19	to	to	PART
eurjchem-193	109	20	give	give	VERB
eurjchem-193	109	21	compound	compound	NOUN
eurjchem-193	109	22	9	9	NUM
eurjchem-193	109	23	as	as	ADP
eurjchem-193	109	24	orange	orange	ADJ
eurjchem-193	109	25	crystals	crystal	NOUN
eurjchem-193	109	26	(	(	PUNCT
eurjchem-193	109	27	scheme	scheme	NOUN
eurjchem-193	109	28	3	3	NUM
eurjchem-193	109	29	)	)	PUNCT
eurjchem-193	109	30	.	.	PUNCT
eurjchem-193	110	1	yield	yield	NOUN
eurjchem-193	110	2	:	:	PUNCT
eurjchem-193	110	3	32	32	NUM
eurjchem-193	110	4	%	%	NOUN
eurjchem-193	110	5	.	.	PUNCT
eurjchem-193	111	1	m.p	m.p	PROPN
eurjchem-193	111	2	.	.	PROPN
eurjchem-193	111	3	:	:	PUNCT
eurjchem-193	112	1	164‐166	164‐166	NUM
eurjchem-193	112	2	°	°	ADP
eurjchem-193	112	3	c	c	X
eurjchem-193	112	4	.	.	PUNCT
eurjchem-193	113	1	ft‐ir	ft‐ir	NOUN
eurjchem-193	113	2	(	(	PUNCT
eurjchem-193	113	3	kbr	kbr	PROPN
eurjchem-193	113	4	,	,	PUNCT
eurjchem-193	113	5	cm‐1	cm‐1	PROPN
eurjchem-193	113	6	):	):	PUNCT
eurjchem-193	113	7	br	br	PROPN
eurjchem-193	113	8	.	.	PUNCT
eurjchem-193	113	9	centered	center	VERB
eurjchem-193	113	10	at	at	ADP
eurjchem-193	113	11	3446	3446	NUM
eurjchem-193	113	12	ν(nh	ν(nh	NOUN
eurjchem-193	113	13	,	,	PUNCT
eurjchem-193	113	14	oh	oh	INTJ
eurjchem-193	113	15	)	)	PUNCT
eurjchem-193	113	16	,	,	PUNCT
eurjchem-193	113	17	2935	2935	NUM
eurjchem-193	113	18	,	,	PUNCT
eurjchem-193	113	19	2846	2846	NUM
eurjchem-193	113	20	ν(c‐halkyl	ν(c‐halkyl	NOUN
eurjchem-193	113	21	.	.	PUNCT
eurjchem-193	113	22	)	)	PUNCT
eurjchem-193	113	23	,	,	PUNCT
eurjchem-193	113	24	1694	1694	NUM
eurjchem-193	113	25	ν(co	ν(co	NUM
eurjchem-193	113	26	)	)	PUNCT
eurjchem-193	113	27	,	,	PUNCT
eurjchem-193	113	28	1583	1583	NUM
eurjchem-193	113	29	ν(c	ν(c	NOUN
eurjchem-193	113	30	=	=	SYM
eurjchem-193	113	31	c	c	NOUN
eurjchem-193	113	32	)	)	PUNCT
eurjchem-193	113	33	.	.	PUNCT
eurjchem-193	114	1	1h	1h	NUM
eurjchem-193	114	2	nmr	nmr	NOUN
eurjchem-193	114	3	(	(	PUNCT
eurjchem-193	114	4	200	200	NUM
eurjchem-193	114	5	mhz	mhz	NOUN
eurjchem-193	114	6	,	,	PUNCT
eurjchem-193	114	7	cdcl3	cdcl3	NOUN
eurjchem-193	114	8	,	,	PUNCT
eurjchem-193	114	9	ppm	ppm	NOUN
eurjchem-193	114	10	):	):	PUNCT
eurjchem-193	114	11	10.2	10.2	NUM
eurjchem-193	114	12	(	(	PUNCT
eurjchem-193	114	13	s	s	PROPN
eurjchem-193	114	14	,	,	PUNCT
eurjchem-193	114	15	2h	2h	NUM
eurjchem-193	114	16	,	,	PUNCT
eurjchem-193	114	17	2cooh	2cooh	NUM
eurjchem-193	114	18	,	,	PUNCT
eurjchem-193	114	19	exchangeable	exchangeable	ADJ
eurjchem-193	114	20	with	with	ADP
eurjchem-193	114	21	d2o	d2o	NOUN
eurjchem-193	114	22	)	)	PUNCT
eurjchem-193	114	23	,	,	PUNCT
eurjchem-193	114	24	7.53	7.53	NUM
eurjchem-193	114	25	(	(	PUNCT
eurjchem-193	114	26	s	s	PROPN
eurjchem-193	114	27	,	,	PUNCT
eurjchem-193	114	28	1h	1h	NUM
eurjchem-193	114	29	,	,	PUNCT
eurjchem-193	114	30	exchangeable	exchangeable	ADJ
eurjchem-193	114	31	with	with	ADP
eurjchem-193	114	32	d2o	d2o	NOUN
eurjchem-193	114	33	)	)	PUNCT
eurjchem-193	114	34	,	,	PUNCT
eurjchem-193	114	35	7.15	7.15	NUM
eurjchem-193	114	36	(	(	PUNCT
eurjchem-193	114	37	s	s	PROPN
eurjchem-193	114	38	,	,	PUNCT
eurjchem-193	114	39	1h	1h	NUM
eurjchem-193	114	40	,	,	PUNCT
eurjchem-193	114	41	ch=	ch=	NOUN
eurjchem-193	114	42	)	)	PUNCT
eurjchem-193	114	43	,	,	PUNCT
eurjchem-193	114	44	6.8	6.8	NUM
eurjchem-193	114	45	(	(	PUNCT
eurjchem-193	114	46	s	s	PROPN
eurjchem-193	114	47	,	,	PUNCT
eurjchem-193	114	48	2harom	2harom	NUM
eurjchem-193	114	49	.	.	PUNCT
eurjchem-193	114	50	)	)	PUNCT
eurjchem-193	114	51	,	,	PUNCT
eurjchem-193	114	52	4.77	4.77	NUM
eurjchem-193	114	53	(	(	PUNCT
eurjchem-193	114	54	s	s	PROPN
eurjchem-193	114	55	,	,	PUNCT
eurjchem-193	114	56	1h	1h	NUM
eurjchem-193	114	57	)	)	PUNCT
eurjchem-193	114	58	,	,	PUNCT
eurjchem-193	114	59	3.9‐3.8	3.9‐3.8	NUM
eurjchem-193	114	60	(	(	PUNCT
eurjchem-193	114	61	two	two	NUM
eurjchem-193	114	62	s	s	NOUN
eurjchem-193	114	63	,	,	PUNCT
eurjchem-193	114	64	9h	9h	NUM
eurjchem-193	114	65	,	,	PUNCT
eurjchem-193	114	66	3ome	3ome	NUM
eurjchem-193	114	67	)	)	PUNCT
eurjchem-193	114	68	,	,	PUNCT
eurjchem-193	114	69	1.6‐1.07	1.6‐1.07	NUM
eurjchem-193	114	70	(	(	PUNCT
eurjchem-193	114	71	m	m	PROPN
eurjchem-193	114	72	,	,	PUNCT
eurjchem-193	114	73	10h	10h	NUM
eurjchem-193	114	74	,	,	PUNCT
eurjchem-193	114	75	c5h10n	c5h10n	PROPN
eurjchem-193	114	76	)	)	PUNCT
eurjchem-193	114	77	.	.	PUNCT
eurjchem-193	115	1	ms	ms	NOUN
eurjchem-193	115	2	(	(	PUNCT
eurjchem-193	115	3	ei	ei	PROPN
eurjchem-193	115	4	,	,	PUNCT
eurjchem-193	115	5	m	m	PROPN
eurjchem-193	115	6	/	/	SYM
eurjchem-193	115	7	z	z	PROPN
eurjchem-193	115	8	(	(	PUNCT
eurjchem-193	115	9	%	%	NOUN
eurjchem-193	115	10	)	)	PUNCT
eurjchem-193	115	11	):	):	PUNCT
eurjchem-193	115	12	466	466	NUM
eurjchem-193	115	13	(	(	PUNCT
eurjchem-193	115	14	m	m	PROPN
eurjchem-193	115	15	,	,	PUNCT
eurjchem-193	115	16	10.2	10.2	NUM
eurjchem-193	115	17	)	)	PUNCT
eurjchem-193	115	18	,	,	PUNCT
eurjchem-193	115	19	462	462	NUM
eurjchem-193	115	20	(	(	PUNCT
eurjchem-193	115	21	m‐2h2	m‐2h2	PROPN
eurjchem-193	115	22	,	,	PUNCT
eurjchem-193	115	23	23.6	23.6	NUM
eurjchem-193	115	24	)	)	PUNCT
eurjchem-193	115	25	,	,	PUNCT
eurjchem-193	115	26	323	323	NUM
eurjchem-193	115	27	(	(	PUNCT
eurjchem-193	115	28	base	base	NOUN
eurjchem-193	115	29	,	,	PUNCT
eurjchem-193	115	30	100	100	NUM
eurjchem-193	115	31	)	)	PUNCT
eurjchem-193	115	32	,	,	PUNCT
eurjchem-193	115	33	224	224	NUM
eurjchem-193	115	34	(	(	PUNCT
eurjchem-193	115	35	17.6	17.6	NUM
eurjchem-193	115	36	)	)	PUNCT
eurjchem-193	115	37	,	,	PUNCT
eurjchem-193	115	38	210	210	NUM
eurjchem-193	115	39	(	(	PUNCT
eurjchem-193	115	40	16.9	16.9	NUM
eurjchem-193	115	41	)	)	PUNCT
eurjchem-193	115	42	.	.	PUNCT
eurjchem-193	116	1	anal	anal	PROPN
eurjchem-193	116	2	.	.	PUNCT
eurjchem-193	116	3	calcd	calcd	NOUN
eurjchem-193	116	4	.	.	PUNCT
eurjchem-193	117	1	for	for	SCONJ
eurjchem-193	117	2	c21h26n2o8s	c21h26n2o8s	NUM
eurjchem-193	117	3	(	(	PUNCT
eurjchem-193	117	4	466.48	466.48	NUM
eurjchem-193	117	5	):	):	PUNCT
eurjchem-193	117	6	c	c	X
eurjchem-193	117	7	,	,	PUNCT
eurjchem-193	117	8	54.18	54.18	NUM
eurjchem-193	117	9	;	;	PUNCT
eurjchem-193	117	10	h	h	NOUN
eurjchem-193	117	11	,	,	PUNCT
eurjchem-193	117	12	5.4	5.4	NUM
eurjchem-193	117	13	;	;	PUNCT
eurjchem-193	117	14	n	n	CCONJ
eurjchem-193	117	15	,	,	PUNCT
eurjchem-193	117	16	6.01	6.01	NUM
eurjchem-193	117	17	.	.	PUNCT
eurjchem-193	117	18	found	find	VERB
eurjchem-193	117	19	:	:	PUNCT
eurjchem-193	118	1	c	c	X
eurjchem-193	118	2	,	,	PUNCT
eurjchem-193	118	3	54.6	54.6	NUM
eurjchem-193	118	4	;	;	PUNCT
eurjchem-193	118	5	h	h	NOUN
eurjchem-193	118	6	,	,	PUNCT
eurjchem-193	118	7	5.34	5.34	NUM
eurjchem-193	118	8	;	;	PUNCT
eurjchem-193	118	9	n	n	CCONJ
eurjchem-193	118	10	,	,	PUNCT
eurjchem-193	118	11	5.92	5.92	NUM
eurjchem-193	118	12	%	%	NOUN
eurjchem-193	118	13	.	.	PUNCT
eurjchem-193	119	1	(	(	PUNCT
eurjchem-193	119	2	z)‐5‐(3,4,5‐trimethoxybenzylidene)‐3h‐thiazolidin‐2,4‐dione	z)‐5‐(3,4,5‐trimethoxybenzylidene)‐3h‐thiazolidin‐2,4‐dione	NOUN
eurjchem-193	119	3	potassium	potassium	NOUN
eurjchem-193	119	4	salt	salt	NOUN
eurjchem-193	119	5	(	(	PUNCT
eurjchem-193	119	6	10	10	NUM
eurjchem-193	119	7	):	):	PUNCT
eurjchem-193	119	8	a	a	DET
eurjchem-193	119	9	mixture	mixture	NOUN
eurjchem-193	119	10	of	of	ADP
eurjchem-193	119	11	6	6	NUM
eurjchem-193	119	12	(	(	PUNCT
eurjchem-193	119	13	5	5	NUM
eurjchem-193	119	14	mmole	mmole	NOUN
eurjchem-193	119	15	)	)	PUNCT
eurjchem-193	119	16	and	and	CCONJ
eurjchem-193	119	17	25	25	NUM
eurjchem-193	119	18	ml	ml	NUM
eurjchem-193	119	19	10	10	NUM
eurjchem-193	119	20	%	%	NOUN
eurjchem-193	119	21	ethanolic	ethanolic	ADJ
eurjchem-193	119	22	potassium	potassium	NOUN
eurjchem-193	119	23	hydroxide	hydroxide	NOUN
eurjchem-193	119	24	solution	solution	NOUN
eurjchem-193	119	25	was	be	AUX
eurjchem-193	119	26	refluxed	refluxe	VERB
eurjchem-193	119	27	for	for	ADP
eurjchem-193	119	28	1h	1h	NUM
eurjchem-193	119	29	.	.	PUNCT
eurjchem-193	120	1	after	after	ADP
eurjchem-193	120	2	concentration	concentration	NOUN
eurjchem-193	120	3	the	the	DET
eurjchem-193	120	4	separated	separated	ADJ
eurjchem-193	120	5	potassium	potassium	NOUN
eurjchem-193	120	6	salt	salt	NOUN
eurjchem-193	120	7	was	be	AUX
eurjchem-193	120	8	collected	collect	VERB
eurjchem-193	120	9	by	by	ADP
eurjchem-193	120	10	suction	suction	NOUN
eurjchem-193	120	11	as	as	ADP
eurjchem-193	120	12	white	white	ADJ
eurjchem-193	120	13	crystals	crystal	NOUN
eurjchem-193	120	14	(	(	PUNCT
eurjchem-193	120	15	scheme	scheme	NOUN
eurjchem-193	120	16	3	3	NUM
eurjchem-193	120	17	)	)	PUNCT
eurjchem-193	120	18	.	.	PUNCT
eurjchem-193	121	1	yield	yield	NOUN
eurjchem-193	121	2	:	:	PUNCT
eurjchem-193	121	3	80	80	NUM
eurjchem-193	121	4	%	%	NOUN
eurjchem-193	121	5	.	.	PUNCT
eurjchem-193	122	1	m.p	m.p	PROPN
eurjchem-193	122	2	.	.	PROPN
eurjchem-193	122	3	:	:	PUNCT
eurjchem-193	123	1	>	>	PUNCT
eurjchem-193	123	2	300	300	NUM
eurjchem-193	123	3	°	°	SYM
eurjchem-193	123	4	c	c	NOUN
eurjchem-193	123	5	.	.	PUNCT
eurjchem-193	124	1	ft‐ir	ft‐ir	NOUN
eurjchem-193	124	2	(	(	PUNCT
eurjchem-193	124	3	kbr	kbr	PROPN
eurjchem-193	124	4	,	,	PUNCT
eurjchem-193	124	5	cm‐1	cm‐1	PROPN
eurjchem-193	124	6	):	):	PUNCT
eurjchem-193	124	7	3077	3077	NUM
eurjchem-193	124	8	ν(c‐harom	ν(c‐harom	NOUN
eurjchem-193	124	9	.	.	PUNCT
eurjchem-193	124	10	)	)	PUNCT
eurjchem-193	124	11	,	,	PUNCT
eurjchem-193	124	12	2946	2946	NUM
eurjchem-193	124	13	ν(c‐halkyl	ν(c‐halkyl	NOUN
eurjchem-193	124	14	.	.	PUNCT
eurjchem-193	124	15	)	)	PUNCT
eurjchem-193	124	16	,	,	PUNCT
eurjchem-193	124	17	1652	1652	NUM
eurjchem-193	124	18	ν(co	ν(co	NOUN
eurjchem-193	124	19	)	)	PUNCT
eurjchem-193	124	20	.	.	PUNCT
eurjchem-193	125	1	1h	1h	NUM
eurjchem-193	125	2	nmr	nmr	NOUN
eurjchem-193	125	3	(	(	PUNCT
eurjchem-193	125	4	200	200	NUM
eurjchem-193	125	5	mhz	mhz	NOUN
eurjchem-193	125	6	,	,	PUNCT
eurjchem-193	125	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-193	125	8	,	,	PUNCT
eurjchem-193	125	9	ppm	ppm	NOUN
eurjchem-193	125	10	):	):	PUNCT
eurjchem-193	125	11	7.84	7.84	NUM
eurjchem-193	125	12	(	(	PUNCT
eurjchem-193	125	13	s	s	PROPN
eurjchem-193	125	14	,	,	PUNCT
eurjchem-193	125	15	2harom	2harom	NUM
eurjchem-193	125	16	.	.	PUNCT
eurjchem-193	125	17	)	)	PUNCT
eurjchem-193	125	18	,	,	PUNCT
eurjchem-193	125	19	7.66	7.66	NUM
eurjchem-193	125	20	(	(	PUNCT
eurjchem-193	125	21	s	s	PROPN
eurjchem-193	125	22	,	,	PUNCT
eurjchem-193	125	23	1h	1h	NUM
eurjchem-193	125	24	,	,	PUNCT
eurjchem-193	125	25	ch=	ch=	NOUN
eurjchem-193	125	26	)	)	PUNCT
eurjchem-193	125	27	,	,	PUNCT
eurjchem-193	125	28	3.9‐3.8	3.9‐3.8	NUM
eurjchem-193	125	29	(	(	PUNCT
eurjchem-193	125	30	two	two	NUM
eurjchem-193	125	31	s	s	NOUN
eurjchem-193	125	32	,	,	PUNCT
eurjchem-193	125	33	9h	9h	NUM
eurjchem-193	125	34	,	,	PUNCT
eurjchem-193	125	35	3ome	3ome	NUM
eurjchem-193	125	36	)	)	PUNCT
eurjchem-193	125	37	.	.	PUNCT
eurjchem-193	126	1	(	(	PUNCT
eurjchem-193	126	2	z)‐5‐(3,4,5‐trimethoxybenzylidene)‐3h‐thiazolidin‐2,4‐dione	z)‐5‐(3,4,5‐trimethoxybenzylidene)‐3h‐thiazolidin‐2,4‐dione	NOUN
eurjchem-193	126	3	(	(	PUNCT
eurjchem-193	126	4	11	11	NUM
eurjchem-193	126	5	):	):	PUNCT
eurjchem-193	126	6	the	the	DET
eurjchem-193	126	7	potassium	potassium	NOUN
eurjchem-193	126	8	salt	salt	NOUN
eurjchem-193	126	9	10	10	NUM
eurjchem-193	126	10	was	be	AUX
eurjchem-193	126	11	dissolved	dissolve	VERB
eurjchem-193	126	12	in	in	ADP
eurjchem-193	126	13	water	water	NOUN
eurjchem-193	126	14	with	with	ADP
eurjchem-193	126	15	stirring	stir	VERB
eurjchem-193	126	16	then	then	ADV
eurjchem-193	126	17	acidified	acidify	VERB
eurjchem-193	126	18	with	with	ADP
eurjchem-193	126	19	acetic	acetic	ADJ
eurjchem-193	126	20	acid	acid	NOUN
eurjchem-193	126	21	.	.	PUNCT
eurjchem-193	127	1	the	the	DET
eurjchem-193	127	2	solid	solid	ADJ
eurjchem-193	127	3	deposited	deposit	VERB
eurjchem-193	127	4	was	be	AUX
eurjchem-193	127	5	filtered	filter	VERB
eurjchem-193	127	6	off	off	ADP
eurjchem-193	127	7	,	,	PUNCT
eurjchem-193	127	8	washed	wash	VERB
eurjchem-193	127	9	several	several	ADJ
eurjchem-193	127	10	times	time	NOUN
eurjchem-193	127	11	with	with	ADP
eurjchem-193	127	12	water	water	NOUN
eurjchem-193	127	13	,	,	PUNCT
eurjchem-193	127	14	dried	dry	VERB
eurjchem-193	127	15	and	and	CCONJ
eurjchem-193	127	16	then	then	ADV
eurjchem-193	127	17	recrystallized	recrystallize	VERB
eurjchem-193	127	18	from	from	ADP
eurjchem-193	127	19	dilute	dilute	NOUN
eurjchem-193	127	20	ethanol	ethanol	NOUN
eurjchem-193	127	21	as	as	ADP
eurjchem-193	127	22	pale	pale	ADJ
eurjchem-193	127	23	yellow	yellow	ADJ
eurjchem-193	127	24	crystals	crystal	NOUN
eurjchem-193	127	25	(	(	PUNCT
eurjchem-193	127	26	scheme	scheme	NOUN
eurjchem-193	127	27	3	3	NUM
eurjchem-193	127	28	)	)	PUNCT
eurjchem-193	127	29	.	.	PUNCT
eurjchem-193	128	1	yield	yield	NOUN
eurjchem-193	128	2	:	:	PUNCT
eurjchem-193	128	3	90	90	NUM
eurjchem-193	128	4	%	%	NOUN
eurjchem-193	128	5	.	.	PUNCT
eurjchem-193	129	1	m.p	m.p	PROPN
eurjchem-193	129	2	.	.	PROPN
eurjchem-193	129	3	:	:	PUNCT
eurjchem-193	130	1	207‐208	207‐208	NUM
eurjchem-193	130	2	°	°	PROPN
eurjchem-193	130	3	c	c	NOUN
eurjchem-193	130	4	.	.	PUNCT
eurjchem-193	130	5	ft‐ir	ft‐ir	NOUN
eurjchem-193	130	6	(	(	PUNCT
eurjchem-193	130	7	kbr	kbr	PROPN
eurjchem-193	130	8	,	,	PUNCT
eurjchem-193	130	9	cm‐1	cm‐1	PROPN
eurjchem-193	130	10	):	):	PUNCT
eurjchem-193	130	11	3127	3127	NUM
eurjchem-193	130	12	ν(nh	ν(nh	NOUN
eurjchem-193	130	13	)	)	PUNCT
eurjchem-193	130	14	,	,	PUNCT
eurjchem-193	130	15	2931	2931	NUM
eurjchem-193	130	16	,	,	PUNCT
eurjchem-193	130	17	2852	2852	NUM
eurjchem-193	130	18	ν(c‐halkyl	ν(c‐halkyl	NOUN
eurjchem-193	130	19	.	.	PUNCT
eurjchem-193	130	20	)	)	PUNCT
eurjchem-193	130	21	,	,	PUNCT
eurjchem-193	130	22	1737	1737	NUM
eurjchem-193	130	23	,	,	PUNCT
eurjchem-193	130	24	1680	1680	NUM
eurjchem-193	130	25	ν(co	ν(co	NUM
eurjchem-193	130	26	)	)	PUNCT
eurjchem-193	130	27	.	.	PUNCT
eurjchem-193	131	1	1h	1h	NUM
eurjchem-193	131	2	nmr	nmr	NOUN
eurjchem-193	131	3	(	(	PUNCT
eurjchem-193	131	4	200	200	NUM
eurjchem-193	131	5	mhz	mhz	NOUN
eurjchem-193	131	6	,	,	PUNCT
eurjchem-193	131	7	cdcl3	cdcl3	NOUN
eurjchem-193	131	8	,	,	PUNCT
eurjchem-193	131	9	ppm	ppm	NUM
eurjchem-193	131	10	):	):	PUNCT
eurjchem-193	131	11	10.7	10.7	NUM
eurjchem-193	131	12	(	(	PUNCT
eurjchem-193	131	13	s	s	PROPN
eurjchem-193	131	14	,	,	PUNCT
eurjchem-193	131	15	1h	1h	NUM
eurjchem-193	131	16	,	,	PUNCT
eurjchem-193	131	17	exchangeable	exchangeable	ADJ
eurjchem-193	131	18	with	with	ADP
eurjchem-193	131	19	d2o	d2o	NOUN
eurjchem-193	131	20	)	)	PUNCT
eurjchem-193	131	21	,	,	PUNCT
eurjchem-193	131	22	8.03	8.03	NUM
eurjchem-193	131	23	(	(	PUNCT
eurjchem-193	131	24	s	s	PROPN
eurjchem-193	131	25	,	,	PUNCT
eurjchem-193	131	26	1h	1h	NUM
eurjchem-193	131	27	,	,	PUNCT
eurjchem-193	131	28	ch=	ch=	NOUN
eurjchem-193	131	29	)	)	PUNCT
eurjchem-193	131	30	,	,	PUNCT
eurjchem-193	131	31	6.78	6.78	NUM
eurjchem-193	131	32	(	(	PUNCT
eurjchem-193	131	33	s	s	PROPN
eurjchem-193	131	34	,	,	PUNCT
eurjchem-193	131	35	2harom	2harom	NUM
eurjchem-193	131	36	.	.	PUNCT
eurjchem-193	131	37	)	)	PUNCT
eurjchem-193	131	38	,	,	PUNCT
eurjchem-193	131	39	3.9‐3.8	3.9‐3.8	NUM
eurjchem-193	131	40	(	(	PUNCT
eurjchem-193	131	41	two	two	NUM
eurjchem-193	131	42	s	s	NOUN
eurjchem-193	131	43	,	,	PUNCT
eurjchem-193	131	44	9h	9h	NUM
eurjchem-193	131	45	,	,	PUNCT
eurjchem-193	131	46	3ome	3ome	NUM
eurjchem-193	131	47	)	)	PUNCT
eurjchem-193	131	48	.	.	PUNCT
eurjchem-193	132	1	ms	ms	NOUN
eurjchem-193	132	2	(	(	PUNCT
eurjchem-193	132	3	ei	ei	PROPN
eurjchem-193	132	4	,	,	PUNCT
eurjchem-193	132	5	m	m	PROPN
eurjchem-193	132	6	/	/	SYM
eurjchem-193	132	7	z	z	PROPN
eurjchem-193	132	8	(	(	PUNCT
eurjchem-193	132	9	%	%	NOUN
eurjchem-193	132	10	)	)	PUNCT
eurjchem-193	132	11	):	):	PUNCT
eurjchem-193	132	12	295	295	NUM
eurjchem-193	132	13	(	(	PUNCT
eurjchem-193	132	14	m	m	PROPN
eurjchem-193	132	15	,	,	PUNCT
eurjchem-193	132	16	32.3	32.3	NUM
eurjchem-193	132	17	)	)	PUNCT
eurjchem-193	132	18	,	,	PUNCT
eurjchem-193	132	19	224	224	NUM
eurjchem-193	132	20	(	(	PUNCT
eurjchem-193	132	21	base	base	NOUN
eurjchem-193	132	22	,	,	PUNCT
eurjchem-193	132	23	100	100	NUM
eurjchem-193	132	24	)	)	PUNCT
eurjchem-193	132	25	,	,	PUNCT
eurjchem-193	132	26	134	134	NUM
eurjchem-193	132	27	(	(	PUNCT
eurjchem-193	132	28	base‐3ch2o	base‐3ch2o	NOUN
eurjchem-193	132	29	,	,	PUNCT
eurjchem-193	132	30	16.8	16.8	NUM
eurjchem-193	132	31	)	)	PUNCT
eurjchem-193	132	32	,	,	PUNCT
eurjchem-193	132	33	91	91	NUM
eurjchem-193	132	34	(	(	PUNCT
eurjchem-193	132	35	11.7	11.7	NUM
eurjchem-193	132	36	)	)	PUNCT
eurjchem-193	132	37	,	,	PUNCT
eurjchem-193	132	38	77	77	NUM
eurjchem-193	132	39	(	(	PUNCT
eurjchem-193	132	40	28.6	28.6	NUM
eurjchem-193	132	41	)	)	PUNCT
eurjchem-193	132	42	,	,	PUNCT
eurjchem-193	132	43	65	65	NUM
eurjchem-193	132	44	(	(	PUNCT
eurjchem-193	132	45	55.3	55.3	NUM
eurjchem-193	132	46	)	)	PUNCT
eurjchem-193	132	47	.	.	PUNCT
eurjchem-193	133	1	anal	anal	PROPN
eurjchem-193	133	2	.	.	PUNCT
eurjchem-193	133	3	calcd	calcd	NOUN
eurjchem-193	133	4	.	.	PUNCT
eurjchem-193	134	1	for	for	ADP
eurjchem-193	134	2	c13h13no5s	c13h13no5s	PROPN
eurjchem-193	134	3	(	(	PUNCT
eurjchem-193	134	4	295.29	295.29	NUM
eurjchem-193	134	5	):	):	PUNCT
eurjchem-193	134	6	c	c	X
eurjchem-193	134	7	,	,	PUNCT
eurjchem-193	134	8	52.87	52.87	NUM
eurjchem-193	134	9	;	;	PUNCT
eurjchem-193	134	10	h	h	NOUN
eurjchem-193	134	11	,	,	PUNCT
eurjchem-193	134	12	4.43	4.43	NUM
eurjchem-193	134	13	;	;	PUNCT
eurjchem-193	134	14	n	n	CCONJ
eurjchem-193	134	15	,	,	PUNCT
eurjchem-193	134	16	4.74	4.74	NUM
eurjchem-193	134	17	.	.	PUNCT
eurjchem-193	134	18	found	find	VERB
eurjchem-193	134	19	:	:	PUNCT
eurjchem-193	135	1	c	c	X
eurjchem-193	135	2	,	,	PUNCT
eurjchem-193	135	3	53.42	53.42	NUM
eurjchem-193	135	4	;	;	PUNCT
eurjchem-193	135	5	h	h	NOUN
eurjchem-193	135	6	,	,	PUNCT
eurjchem-193	135	7	4.4	4.4	NUM
eurjchem-193	135	8	;	;	PUNCT
eurjchem-193	135	9	n	n	CCONJ
eurjchem-193	135	10	,	,	PUNCT
eurjchem-193	135	11	4.66	4.66	NUM
eurjchem-193	135	12	%	%	NOUN
eurjchem-193	135	13	.	.	PUNCT
eurjchem-193	136	1	478	478	NUM
eurjchem-193	136	2	madmoud	madmoud	PROPN
eurjchem-193	136	3	et	et	PROPN
eurjchem-193	136	4	al	al	PROPN
eurjchem-193	136	5	.	.	PUNCT
eurjchem-193	136	6	/	/	SYM
eurjchem-193	136	7	european	european	PROPN
eurjchem-193	136	8	journal	journal	PROPN
eurjchem-193	136	9	of	of	ADP
eurjchem-193	136	10	chemistry	chemistry	NOUN
eurjchem-193	136	11	2	2	NUM
eurjchem-193	136	12	(	(	PUNCT
eurjchem-193	136	13	4	4	NUM
eurjchem-193	136	14	)	)	PUNCT
eurjchem-193	136	15	(	(	PUNCT
eurjchem-193	136	16	2011	2011	NUM
eurjchem-193	136	17	)	)	PUNCT
eurjchem-193	136	18	475‐479	475‐479	NUM
eurjchem-193	136	19	scheme	scheme	NOUN
eurjchem-193	136	20	4	4	NUM
eurjchem-193	136	21	(	(	PUNCT
eurjchem-193	136	22	z)ethyl‐2‐[2,4‐dioxo‐5‐(3,4,5‐trimethoxybenzylidene)‐	z)ethyl‐2‐[2,4‐dioxo‐5‐(3,4,5‐trimethoxybenzylidene)‐	X
eurjchem-193	136	23	thiazolidin‐3‐yl]acetate	thiazolidin‐3‐yl]acetate	NOUN
eurjchem-193	136	24	(	(	PUNCT
eurjchem-193	136	25	12	12	NUM
eurjchem-193	136	26	):	):	PUNCT
eurjchem-193	136	27	a	a	DET
eurjchem-193	136	28	mixture	mixture	NOUN
eurjchem-193	136	29	of	of	ADP
eurjchem-193	136	30	10	10	NUM
eurjchem-193	136	31	(	(	PUNCT
eurjchem-193	136	32	1.67	1.67	NUM
eurjchem-193	136	33	g	g	NOUN
eurjchem-193	136	34	,	,	PUNCT
eurjchem-193	136	35	5	5	NUM
eurjchem-193	136	36	mmole	mmole	NOUN
eurjchem-193	136	37	)	)	PUNCT
eurjchem-193	136	38	and	and	CCONJ
eurjchem-193	136	39	ethylchloroacetate	ethylchloroacetate	NOUN
eurjchem-193	136	40	(	(	PUNCT
eurjchem-193	136	41	0.62	0.62	NUM
eurjchem-193	136	42	g	g	NOUN
eurjchem-193	136	43	,	,	PUNCT
eurjchem-193	136	44	5	5	NUM
eurjchem-193	136	45	mmole	mmole	NOUN
eurjchem-193	136	46	)	)	PUNCT
eurjchem-193	136	47	was	be	AUX
eurjchem-193	136	48	refluxed	refluxe	VERB
eurjchem-193	136	49	in	in	ADP
eurjchem-193	136	50	30	30	NUM
eurjchem-193	136	51	ml	ml	NOUN
eurjchem-193	136	52	ethanol	ethanol	NOUN
eurjchem-193	136	53	for	for	ADP
eurjchem-193	136	54	6	6	NUM
eurjchem-193	136	55	hrs	hrs	NOUN
eurjchem-193	136	56	(	(	PUNCT
eurjchem-193	136	57	tlc	tlc	NOUN
eurjchem-193	136	58	)	)	PUNCT
eurjchem-193	136	59	.	.	PUNCT
eurjchem-193	137	1	the	the	DET
eurjchem-193	137	2	separated	separate	VERB
eurjchem-193	137	3	solid	solid	ADJ
eurjchem-193	137	4	was	be	AUX
eurjchem-193	137	5	filtered	filter	VERB
eurjchem-193	137	6	off	off	ADP
eurjchem-193	137	7	,	,	PUNCT
eurjchem-193	137	8	dried	dry	VERB
eurjchem-193	137	9	and	and	CCONJ
eurjchem-193	137	10	then	then	ADV
eurjchem-193	137	11	recrystallized	recrystallize	VERB
eurjchem-193	137	12	from	from	ADP
eurjchem-193	137	13	ethanol	ethanol	NOUN
eurjchem-193	137	14	to	to	PART
eurjchem-193	137	15	give	give	VERB
eurjchem-193	137	16	compound	compound	NOUN
eurjchem-193	137	17	12	12	NUM
eurjchem-193	137	18	as	as	ADP
eurjchem-193	137	19	pale	pale	ADJ
eurjchem-193	137	20	yellow	yellow	ADJ
eurjchem-193	137	21	crystals	crystal	NOUN
eurjchem-193	137	22	(	(	PUNCT
eurjchem-193	137	23	scheme	scheme	NOUN
eurjchem-193	137	24	3	3	NUM
eurjchem-193	137	25	)	)	PUNCT
eurjchem-193	137	26	.	.	PUNCT
eurjchem-193	138	1	yield	yield	NOUN
eurjchem-193	138	2	:	:	PUNCT
eurjchem-193	138	3	23	23	NUM
eurjchem-193	138	4	%	%	NOUN
eurjchem-193	138	5	.	.	PUNCT
eurjchem-193	139	1	m.p	m.p	PROPN
eurjchem-193	139	2	.	.	PROPN
eurjchem-193	139	3	:	:	PUNCT
eurjchem-193	140	1	119	119	NUM
eurjchem-193	140	2	°	°	SYM
eurjchem-193	140	3	c	c	X
eurjchem-193	140	4	.	.	PUNCT
eurjchem-193	140	5	ft‐ir	ft‐ir	NOUN
eurjchem-193	140	6	(	(	PUNCT
eurjchem-193	140	7	kbr	kbr	PROPN
eurjchem-193	140	8	,	,	PUNCT
eurjchem-193	140	9	cm‐1	cm‐1	PROPN
eurjchem-193	140	10	):	):	PUNCT
eurjchem-193	140	11	3072	3072	NUM
eurjchem-193	140	12	ν(c‐harom	ν(c‐harom	NOUN
eurjchem-193	140	13	.	.	PROPN
eurjchem-193	140	14	)	)	PUNCT
eurjchem-193	140	15	,	,	PUNCT
eurjchem-193	140	16	2940	2940	NUM
eurjchem-193	140	17	,	,	PUNCT
eurjchem-193	140	18	2862	2862	NUM
eurjchem-193	140	19	ν(c‐halkyl	ν(c‐halkyl	NOUN
eurjchem-193	140	20	.	.	PUNCT
eurjchem-193	140	21	)	)	PUNCT
eurjchem-193	140	22	,	,	PUNCT
eurjchem-193	140	23	1741	1741	NUM
eurjchem-193	140	24	,	,	PUNCT
eurjchem-193	140	25	1717	1717	NUM
eurjchem-193	140	26	,	,	PUNCT
eurjchem-193	140	27	1682	1682	NUM
eurjchem-193	140	28	ν(co	ν(co	NUM
eurjchem-193	140	29	)	)	PUNCT
eurjchem-193	140	30	.	.	PUNCT
eurjchem-193	141	1	1h	1h	NUM
eurjchem-193	141	2	nmr	nmr	NOUN
eurjchem-193	141	3	(	(	PUNCT
eurjchem-193	141	4	200	200	NUM
eurjchem-193	141	5	mhz	mhz	NOUN
eurjchem-193	141	6	,	,	PUNCT
eurjchem-193	141	7	cdcl3	cdcl3	NOUN
eurjchem-193	141	8	,	,	PUNCT
eurjchem-193	141	9	ppm	ppm	NUM
eurjchem-193	141	10	):	):	PUNCT
eurjchem-193	141	11	7.6	7.6	NUM
eurjchem-193	141	12	(	(	PUNCT
eurjchem-193	141	13	s	s	PROPN
eurjchem-193	141	14	,	,	PUNCT
eurjchem-193	141	15	1h	1h	NUM
eurjchem-193	141	16	,	,	PUNCT
eurjchem-193	141	17	=	=	NOUN
eurjchem-193	141	18	ch	ch	NOUN
eurjchem-193	141	19	)	)	PUNCT
eurjchem-193	141	20	,	,	PUNCT
eurjchem-193	141	21	6.6	6.6	NUM
eurjchem-193	141	22	(	(	PUNCT
eurjchem-193	141	23	s	s	PROPN
eurjchem-193	141	24	,	,	PUNCT
eurjchem-193	141	25	2harom	2harom	NUM
eurjchem-193	141	26	.	.	PUNCT
eurjchem-193	141	27	)	)	PUNCT
eurjchem-193	141	28	,	,	PUNCT
eurjchem-193	141	29	4.6	4.6	NUM
eurjchem-193	141	30	(	(	PUNCT
eurjchem-193	141	31	d	d	NOUN
eurjchem-193	141	32	,	,	PUNCT
eurjchem-193	141	33	d	d	NOUN
eurjchem-193	141	34	,	,	PUNCT
eurjchem-193	141	35	2h	2h	NUM
eurjchem-193	141	36	)	)	PUNCT
eurjchem-193	141	37	,	,	PUNCT
eurjchem-193	141	38	4.2	4.2	NUM
eurjchem-193	141	39	(	(	PUNCT
eurjchem-193	141	40	q	q	NOUN
eurjchem-193	141	41	,	,	PUNCT
eurjchem-193	141	42	2h	2h	NUM
eurjchem-193	141	43	,	,	PUNCT
eurjchem-193	141	44	j	j	PROPN
eurjchem-193	141	45	=	=	PROPN
eurjchem-193	141	46	6.4	6.4	NUM
eurjchem-193	141	47	hz	hz	NOUN
eurjchem-193	141	48	)	)	PUNCT
eurjchem-193	141	49	,	,	PUNCT
eurjchem-193	141	50	3.9‐3.85	3.9‐3.85	NUM
eurjchem-193	141	51	(	(	PUNCT
eurjchem-193	141	52	two	two	NUM
eurjchem-193	141	53	s	s	NOUN
eurjchem-193	141	54	,	,	PUNCT
eurjchem-193	141	55	9h	9h	NUM
eurjchem-193	141	56	,	,	PUNCT
eurjchem-193	141	57	3ome	3ome	NUM
eurjchem-193	141	58	)	)	PUNCT
eurjchem-193	141	59	,	,	PUNCT
eurjchem-193	141	60	1.36	1.36	NUM
eurjchem-193	141	61	(	(	PUNCT
eurjchem-193	141	62	t	t	PROPN
eurjchem-193	141	63	,	,	PUNCT
eurjchem-193	141	64	3h	3h	NUM
eurjchem-193	141	65	,	,	PUNCT
eurjchem-193	141	66	j	j	PROPN
eurjchem-193	141	67	=	=	PROPN
eurjchem-193	141	68	6.4	6.4	NUM
eurjchem-193	141	69	hz	hz	NOUN
eurjchem-193	141	70	)	)	PUNCT
eurjchem-193	141	71	.	.	PUNCT
eurjchem-193	142	1	ms	ms	NOUN
eurjchem-193	142	2	(	(	PUNCT
eurjchem-193	142	3	ei	ei	PROPN
eurjchem-193	142	4	,	,	PUNCT
eurjchem-193	142	5	m	m	PROPN
eurjchem-193	142	6	/	/	SYM
eurjchem-193	142	7	z	z	PROPN
eurjchem-193	142	8	(	(	PUNCT
eurjchem-193	142	9	%	%	NOUN
eurjchem-193	142	10	)	)	PUNCT
eurjchem-193	142	11	):	):	PUNCT
eurjchem-193	142	12	381	381	NUM
eurjchem-193	142	13	(	(	PUNCT
eurjchem-193	142	14	m	m	PROPN
eurjchem-193	142	15	,	,	PUNCT
eurjchem-193	142	16	23.9	23.9	NUM
eurjchem-193	142	17	)	)	PUNCT
eurjchem-193	142	18	,	,	PUNCT
eurjchem-193	142	19	335	335	NUM
eurjchem-193	142	20	(	(	PUNCT
eurjchem-193	142	21	m‐etoh	m‐etoh	ADP
eurjchem-193	142	22	,	,	PUNCT
eurjchem-193	142	23	24.2	24.2	NUM
eurjchem-193	142	24	)	)	PUNCT
eurjchem-193	142	25	,	,	PUNCT
eurjchem-193	142	26	308	308	NUM
eurjchem-193	142	27	(	(	PUNCT
eurjchem-193	142	28	m‐c2h4	m‐c2h4	NOUN
eurjchem-193	142	29	,	,	PUNCT
eurjchem-193	142	30	co2	co2	NOUN
eurjchem-193	142	31	,	,	PUNCT
eurjchem-193	142	32	17.7	17.7	NUM
eurjchem-193	142	33	)	)	PUNCT
eurjchem-193	142	34	,	,	PUNCT
eurjchem-193	142	35	224	224	NUM
eurjchem-193	142	36	(	(	PUNCT
eurjchem-193	142	37	base	base	NOUN
eurjchem-193	142	38	,	,	PUNCT
eurjchem-193	142	39	100	100	NUM
eurjchem-193	142	40	)	)	PUNCT
eurjchem-193	142	41	,	,	PUNCT
eurjchem-193	142	42	134	134	NUM
eurjchem-193	142	43	(	(	PUNCT
eurjchem-193	142	44	base‐3ch2o	base‐3ch2o	NOUN
eurjchem-193	142	45	,	,	PUNCT
eurjchem-193	142	46	7.2	7.2	NUM
eurjchem-193	142	47	)	)	PUNCT
eurjchem-193	142	48	,	,	PUNCT
eurjchem-193	142	49	77	77	NUM
eurjchem-193	142	50	(	(	PUNCT
eurjchem-193	142	51	56.2	56.2	NUM
eurjchem-193	142	52	)	)	PUNCT
eurjchem-193	142	53	.	.	PUNCT
eurjchem-193	143	1	anal	anal	PROPN
eurjchem-193	143	2	.	.	PUNCT
eurjchem-193	143	3	calcd	calcd	NOUN
eurjchem-193	143	4	.	.	PUNCT
eurjchem-193	144	1	for	for	SCONJ
eurjchem-193	144	2	c17h19no7s	c17h19no7s	NOUN
eurjchem-193	144	3	(	(	PUNCT
eurjchem-193	144	4	381.37	381.37	NUM
eurjchem-193	144	5	):	):	PUNCT
eurjchem-193	144	6	c	c	NOUN
eurjchem-193	144	7	,	,	PUNCT
eurjchem-193	144	8	53.53	53.53	NUM
eurjchem-193	144	9	;	;	PUNCT
eurjchem-193	144	10	h	h	NOUN
eurjchem-193	144	11	,	,	PUNCT
eurjchem-193	144	12	5.01	5.01	NUM
eurjchem-193	144	13	;	;	PUNCT
eurjchem-193	144	14	n	n	CCONJ
eurjchem-193	144	15	,	,	PUNCT
eurjchem-193	144	16	3.67	3.67	NUM
eurjchem-193	144	17	.	.	PUNCT
eurjchem-193	144	18	found	find	VERB
eurjchem-193	144	19	:	:	PUNCT
eurjchem-193	145	1	c	c	X
eurjchem-193	145	2	,	,	PUNCT
eurjchem-193	145	3	53.0	53.0	NUM
eurjchem-193	145	4	;	;	PUNCT
eurjchem-193	145	5	h	h	NOUN
eurjchem-193	145	6	,	,	PUNCT
eurjchem-193	145	7	5.17	5.17	NUM
eurjchem-193	145	8	;	;	PUNCT
eurjchem-193	145	9	n	n	CCONJ
eurjchem-193	145	10	,	,	PUNCT
eurjchem-193	145	11	4.07	4.07	NUM
eurjchem-193	145	12	%	%	NOUN
eurjchem-193	145	13	.	.	PUNCT
eurjchem-193	146	1	(	(	PUNCT
eurjchem-193	146	2	z)‐5‐(3,4,5‐trimethoxybenzyli‐dene)‐2‐chloro‐3‐(furan‐2‐	z)‐5‐(3,4,5‐trimethoxybenzyli‐dene)‐2‐chloro‐3‐(furan‐2‐	PROPN
eurjchem-193	146	3	carbonyl)‐4‐oxothiazolidin‐2‐yl	carbonyl)‐4‐oxothiazolidin‐2‐yl	PROPN
eurjchem-193	146	4	furan‐2‐carboxylate	furan‐2‐carboxylate	PROPN
eurjchem-193	146	5	(	(	PUNCT
eurjchem-193	146	6	13	13	NUM
eurjchem-193	146	7	):	):	PUNCT
eurjchem-193	146	8	a	a	DET
eurjchem-193	146	9	mixture	mixture	NOUN
eurjchem-193	146	10	of	of	ADP
eurjchem-193	146	11	10	10	NUM
eurjchem-193	146	12	(	(	PUNCT
eurjchem-193	146	13	1.67	1.67	NUM
eurjchem-193	146	14	g	g	NOUN
eurjchem-193	146	15	,	,	PUNCT
eurjchem-193	146	16	5	5	NUM
eurjchem-193	146	17	mmole	mmole	NOUN
eurjchem-193	146	18	)	)	PUNCT
eurjchem-193	146	19	and	and	CCONJ
eurjchem-193	146	20	furoyl	furoyl	PROPN
eurjchem-193	146	21	chloride	chloride	NOUN
eurjchem-193	146	22	(	(	PUNCT
eurjchem-193	146	23	0.65	0.65	NUM
eurjchem-193	146	24	g	g	NOUN
eurjchem-193	146	25	,	,	PUNCT
eurjchem-193	146	26	5	5	NUM
eurjchem-193	146	27	mmole	mmole	NOUN
eurjchem-193	146	28	)	)	PUNCT
eurjchem-193	146	29	was	be	AUX
eurjchem-193	146	30	refluxed	refluxe	VERB
eurjchem-193	146	31	in	in	ADP
eurjchem-193	146	32	30	30	NUM
eurjchem-193	146	33	ml	ml	NOUN
eurjchem-193	146	34	dry	dry	ADJ
eurjchem-193	146	35	pyridine	pyridine	NOUN
eurjchem-193	146	36	for	for	ADP
eurjchem-193	146	37	4hrs	4hrs	PROPN
eurjchem-193	146	38	(	(	PUNCT
eurjchem-193	146	39	tlc	tlc	NOUN
eurjchem-193	146	40	)	)	PUNCT
eurjchem-193	146	41	.	.	PUNCT
eurjchem-193	147	1	after	after	ADP
eurjchem-193	147	2	concentration	concentration	NOUN
eurjchem-193	147	3	,	,	PUNCT
eurjchem-193	147	4	cold	cold	ADJ
eurjchem-193	147	5	dilute	dilute	NOUN
eurjchem-193	147	6	hydrochloric	hydrochloric	ADJ
eurjchem-193	147	7	acid	acid	NOUN
eurjchem-193	147	8	was	be	AUX
eurjchem-193	147	9	added	add	VERB
eurjchem-193	147	10	.	.	PUNCT
eurjchem-193	148	1	the	the	DET
eurjchem-193	148	2	separated	separate	VERB
eurjchem-193	148	3	solid	solid	ADJ
eurjchem-193	148	4	was	be	AUX
eurjchem-193	148	5	filtered	filter	VERB
eurjchem-193	148	6	off	off	ADP
eurjchem-193	148	7	,	,	PUNCT
eurjchem-193	148	8	washed	wash	VERB
eurjchem-193	148	9	with	with	ADP
eurjchem-193	148	10	water	water	NOUN
eurjchem-193	148	11	,	,	PUNCT
eurjchem-193	148	12	dried	dry	VERB
eurjchem-193	148	13	and	and	CCONJ
eurjchem-193	148	14	then	then	ADV
eurjchem-193	148	15	recrystallized	recrystallize	VERB
eurjchem-193	148	16	from	from	ADP
eurjchem-193	148	17	a	a	DET
eurjchem-193	148	18	mixture	mixture	NOUN
eurjchem-193	148	19	of	of	ADP
eurjchem-193	148	20	benzene	benzene	NOUN
eurjchem-193	148	21	/	/	SYM
eurjchem-193	148	22	ethanol	ethanol	NOUN
eurjchem-193	148	23	to	to	PART
eurjchem-193	148	24	give	give	VERB
eurjchem-193	148	25	compound	compound	NOUN
eurjchem-193	148	26	13	13	NUM
eurjchem-193	148	27	as	as	ADP
eurjchem-193	148	28	yellow	yellow	ADJ
eurjchem-193	148	29	crystals	crystal	NOUN
eurjchem-193	148	30	(	(	PUNCT
eurjchem-193	148	31	scheme	scheme	NOUN
eurjchem-193	148	32	3	3	NUM
eurjchem-193	148	33	)	)	PUNCT
eurjchem-193	148	34	.	.	PUNCT
eurjchem-193	149	1	yield	yield	NOUN
eurjchem-193	149	2	:	:	PUNCT
eurjchem-193	149	3	13	13	NUM
eurjchem-193	149	4	%	%	NOUN
eurjchem-193	149	5	.	.	PUNCT
eurjchem-193	150	1	m.p	m.p	PROPN
eurjchem-193	150	2	.	.	PROPN
eurjchem-193	150	3	:	:	PUNCT
eurjchem-193	151	1	185‐188	185‐188	PROPN
eurjchem-193	151	2	°	°	PROPN
eurjchem-193	151	3	c	c	NOUN
eurjchem-193	151	4	.	.	PUNCT
eurjchem-193	152	1	ft‐ir	ft‐ir	NOUN
eurjchem-193	152	2	(	(	PUNCT
eurjchem-193	152	3	kbr	kbr	PROPN
eurjchem-193	152	4	,	,	PUNCT
eurjchem-193	152	5	cm‐1	cm‐1	PROPN
eurjchem-193	152	6	):	):	PUNCT
eurjchem-193	152	7	3072	3072	NUM
eurjchem-193	152	8	ν(c‐harom	ν(c‐harom	NOUN
eurjchem-193	152	9	.	.	PROPN
eurjchem-193	152	10	)	)	PUNCT
eurjchem-193	152	11	,	,	PUNCT
eurjchem-193	152	12	2935	2935	NUM
eurjchem-193	152	13	,	,	PUNCT
eurjchem-193	152	14	2843	2843	NUM
eurjchem-193	152	15	ν(c‐halkyl	ν(c‐halkyl	NOUN
eurjchem-193	152	16	.	.	PUNCT
eurjchem-193	152	17	)	)	PUNCT
eurjchem-193	152	18	,	,	PUNCT
eurjchem-193	152	19	1717	1717	NUM
eurjchem-193	152	20	ν(coester	ν(coester	NOUN
eurjchem-193	152	21	)	)	PUNCT
eurjchem-193	152	22	,	,	PUNCT
eurjchem-193	152	23	1687	1687	NUM
eurjchem-193	152	24	ν(co	ν(co	NUM
eurjchem-193	152	25	)	)	PUNCT
eurjchem-193	152	26	,	,	PUNCT
eurjchem-193	152	27	1588	1588	NUM
eurjchem-193	152	28	ν(c	ν(c	PROPN
eurjchem-193	152	29	=	=	SYM
eurjchem-193	152	30	c	c	NOUN
eurjchem-193	152	31	)	)	PUNCT
eurjchem-193	152	32	.	.	PUNCT
eurjchem-193	153	1	ms	ms	NOUN
eurjchem-193	153	2	(	(	PUNCT
eurjchem-193	153	3	ei	ei	PROPN
eurjchem-193	153	4	,	,	PUNCT
eurjchem-193	153	5	m	m	PROPN
eurjchem-193	153	6	/	/	SYM
eurjchem-193	153	7	z	z	PROPN
eurjchem-193	153	8	(	(	PUNCT
eurjchem-193	153	9	%	%	NOUN
eurjchem-193	153	10	)	)	PUNCT
eurjchem-193	153	11	):	):	PUNCT
eurjchem-193	153	12	521	521	NUM
eurjchem-193	153	13	(	(	PUNCT
eurjchem-193	153	14	m+2	m+2	NOUN
eurjchem-193	153	15	,	,	PUNCT
eurjchem-193	153	16	9.7	9.7	NUM
eurjchem-193	153	17	)	)	PUNCT
eurjchem-193	153	18	,	,	PUNCT
eurjchem-193	153	19	520	520	NUM
eurjchem-193	153	20	(	(	PUNCT
eurjchem-193	153	21	m	m	PROPN
eurjchem-193	153	22	,	,	PUNCT
eurjchem-193	153	23	27.8	27.8	NUM
eurjchem-193	153	24	)	)	PUNCT
eurjchem-193	153	25	,	,	PUNCT
eurjchem-193	153	26	298	298	NUM
eurjchem-193	153	27	(	(	PUNCT
eurjchem-193	153	28	43.1	43.1	NUM
eurjchem-193	153	29	)	)	PUNCT
eurjchem-193	153	30	,	,	PUNCT
eurjchem-193	153	31	252	252	NUM
eurjchem-193	153	32	(	(	PUNCT
eurjchem-193	153	33	54.9	54.9	NUM
eurjchem-193	153	34	)	)	PUNCT
eurjchem-193	153	35	,	,	PUNCT
eurjchem-193	153	36	224	224	NUM
eurjchem-193	153	37	(	(	PUNCT
eurjchem-193	153	38	base	base	NOUN
eurjchem-193	153	39	,	,	PUNCT
eurjchem-193	153	40	100	100	NUM
eurjchem-193	153	41	)	)	PUNCT
eurjchem-193	153	42	,	,	PUNCT
eurjchem-193	153	43	209	209	NUM
eurjchem-193	153	44	(	(	PUNCT
eurjchem-193	153	45	base‐me	base‐me	ADP
eurjchem-193	153	46	,	,	PUNCT
eurjchem-193	153	47	96.9	96.9	NUM
eurjchem-193	153	48	)	)	PUNCT
eurjchem-193	153	49	.	.	PUNCT
eurjchem-193	154	1	anal	anal	PROPN
eurjchem-193	154	2	.	.	PUNCT
eurjchem-193	154	3	calcd	calcd	NOUN
eurjchem-193	154	4	.	.	PUNCT
eurjchem-193	155	1	for	for	ADP
eurjchem-193	155	2	c23h18clno9s	c23h18clno9	NOUN
eurjchem-193	155	3	(	(	PUNCT
eurjchem-193	155	4	519.89	519.89	NUM
eurjchem-193	155	5	):	):	PUNCT
eurjchem-193	155	6	c	c	NOUN
eurjchem-193	155	7	,	,	PUNCT
eurjchem-193	155	8	53.13	53.13	NUM
eurjchem-193	155	9	;	;	PUNCT
eurjchem-193	155	10	h	h	NOUN
eurjchem-193	155	11	,	,	PUNCT
eurjchem-193	155	12	3.48	3.48	NUM
eurjchem-193	155	13	;	;	PUNCT
eurjchem-193	155	14	n	n	CCONJ
eurjchem-193	155	15	,	,	PUNCT
eurjchem-193	155	16	2.69	2.69	NUM
eurjchem-193	155	17	.	.	PUNCT
eurjchem-193	155	18	found	find	VERB
eurjchem-193	155	19	:	:	PUNCT
eurjchem-193	156	1	c	c	X
eurjchem-193	156	2	,	,	PUNCT
eurjchem-193	156	3	53.42	53.42	NUM
eurjchem-193	156	4	;	;	PUNCT
eurjchem-193	157	1	h	h	NOUN
eurjchem-193	157	2	,	,	PUNCT
eurjchem-193	157	3	3.08	3.08	NUM
eurjchem-193	157	4	;	;	PUNCT
eurjchem-193	157	5	n	n	CCONJ
eurjchem-193	157	6	,	,	PUNCT
eurjchem-193	157	7	3.30	3.30	NUM
eurjchem-193	157	8	%	%	NOUN
eurjchem-193	157	9	.	.	PUNCT
eurjchem-193	158	1	3	3	X
eurjchem-193	158	2	.	.	NOUN
eurjchem-193	158	3	results	result	NOUN
eurjchem-193	158	4	and	and	CCONJ
eurjchem-193	158	5	discussion	discussion	NOUN
eurjchem-193	158	6	5‐arylmethylene‐2‐imino‐4‐oxo‐2‐thiazolidine	5‐arylmethylene‐2‐imino‐4‐oxo‐2‐thiazolidine	PROPN
eurjchem-193	158	7	3	3	NUM
eurjchem-193	158	8	obtained	obtain	VERB
eurjchem-193	158	9	as	as	ADP
eurjchem-193	158	10	the	the	DET
eurjchem-193	158	11	sole	sole	ADJ
eurjchem-193	158	12	product	product	NOUN
eurjchem-193	158	13	in	in	ADP
eurjchem-193	158	14	a	a	DET
eurjchem-193	158	15	good	good	ADJ
eurjchem-193	158	16	yield	yield	NOUN
eurjchem-193	158	17	upon	upon	SCONJ
eurjchem-193	158	18	treatment	treatment	NOUN
eurjchem-193	158	19	of	of	ADP
eurjchem-193	158	20	2‐imino‐	2‐imino‐	NUM
eurjchem-193	158	21	4‐oxo‐2‐thiazolidine	4‐oxo‐2‐thiazolidine	NOUN
eurjchem-193	158	22	(	(	PUNCT
eurjchem-193	158	23	2	2	NUM
eurjchem-193	158	24	)	)	PUNCT
eurjchem-193	158	25	with	with	ADP
eurjchem-193	158	26	α‐cyano‐3,4,5‐trimethoxy	α‐cyano‐3,4,5‐trimethoxy	PROPN
eurjchem-193	158	27	cinna‐	cinna‐	ADV
eurjchem-193	158	28	monnitrile	monnitrile	NOUN
eurjchem-193	158	29	and/or	and/or	CCONJ
eurjchem-193	158	30	ethyl‐α‐cyano‐3,4,5‐trimethoxy	ethyl‐α‐cyano‐3,4,5‐trimethoxy	ADJ
eurjchem-193	158	31	cinnamate	cinnamate	NOUN
eurjchem-193	158	32	(	(	PUNCT
eurjchem-193	158	33	1a	1a	NUM
eurjchem-193	158	34	,	,	PUNCT
eurjchem-193	158	35	b	b	NOUN
eurjchem-193	158	36	)	)	PUNCT
eurjchem-193	158	37	in	in	ADP
eurjchem-193	158	38	refluxing	refluxing	NOUN
eurjchem-193	158	39	ethanol	ethanol	NOUN
eurjchem-193	158	40	in	in	ADP
eurjchem-193	158	41	the	the	DET
eurjchem-193	158	42	presence	presence	NOUN
eurjchem-193	158	43	of	of	ADP
eurjchem-193	158	44	catalytic	catalytic	ADJ
eurjchem-193	158	45	amount	amount	NOUN
eurjchem-193	158	46	of	of	ADP
eurjchem-193	158	47	piperidine	piperidine	NOUN
eurjchem-193	158	48	(	(	PUNCT
eurjchem-193	158	49	scheme	scheme	NOUN
eurjchem-193	158	50	1	1	NUM
eurjchem-193	158	51	)	)	PUNCT
eurjchem-193	158	52	.	.	PUNCT
eurjchem-193	159	1	structure	structure	NOUN
eurjchem-193	159	2	of	of	ADP
eurjchem-193	159	3	compound	compound	NOUN
eurjchem-193	159	4	3	3	NUM
eurjchem-193	159	5	was	be	AUX
eurjchem-193	159	6	substantiated	substantiate	VERB
eurjchem-193	159	7	from	from	ADP
eurjchem-193	159	8	microanalytical	microanalytical	ADJ
eurjchem-193	159	9	data	datum	NOUN
eurjchem-193	159	10	and	and	CCONJ
eurjchem-193	159	11	was	be	AUX
eurjchem-193	159	12	confirmed	confirm	VERB
eurjchem-193	159	13	by	by	ADP
eurjchem-193	159	14	infrared	infrared	PROPN
eurjchem-193	159	15	,	,	PUNCT
eurjchem-193	159	16	1h	1h	NUM
eurjchem-193	159	17	nmr	nmr	NOUN
eurjchem-193	159	18	,	,	PUNCT
eurjchem-193	159	19	13c	13c	NOUN
eurjchem-193	159	20	nmr	nmr	NOUN
eurjchem-193	159	21	and	and	CCONJ
eurjchem-193	159	22	mass	mass	ADJ
eurjchem-193	159	23	spectra	spectra	NOUN
eurjchem-193	159	24	(	(	PUNCT
eurjchem-193	159	25	c.f	c.f	PROPN
eurjchem-193	159	26	.	.	PROPN
eurjchem-193	159	27	exp	exp	PROPN
eurjchem-193	159	28	.	.	PUNCT
eurjchem-193	159	29	)	)	PUNCT
eurjchem-193	159	30	.	.	PUNCT
eurjchem-193	160	1	the	the	DET
eurjchem-193	160	2	configuration	configuration	NOUN
eurjchem-193	160	3	assigned	assign	VERB
eurjchem-193	160	4	to	to	ADP
eurjchem-193	160	5	the	the	DET
eurjchem-193	160	6	exocyclic	exocyclic	ADJ
eurjchem-193	160	7	c	c	NOUN
eurjchem-193	160	8	=	=	NOUN
eurjchem-193	160	9	c	c	NOUN
eurjchem-193	160	10	double	double	ADJ
eurjchem-193	160	11	bond	bond	NOUN
eurjchem-193	160	12	in	in	ADP
eurjchem-193	160	13	compound	compound	NOUN
eurjchem-193	160	14	3	3	NUM
eurjchem-193	160	15	(	(	PUNCT
eurjchem-193	160	16	z‐configuration	z‐configuration	NUM
eurjchem-193	160	17	)	)	PUNCT
eurjchem-193	160	18	has	have	AUX
eurjchem-193	160	19	been	be	AUX
eurjchem-193	160	20	proven	prove	VERB
eurjchem-193	160	21	by	by	ADP
eurjchem-193	160	22	1h	1h	NUM
eurjchem-193	160	23	nmr	nmr	NOUN
eurjchem-193	160	24	calculations	calculation	NOUN
eurjchem-193	160	25	[	[	X
eurjchem-193	160	26	10	10	NUM
eurjchem-193	160	27	]	]	PUNCT
eurjchem-193	160	28	which	which	PRON
eurjchem-193	160	29	are	be	AUX
eurjchem-193	160	30	compatible	compatible	ADJ
eurjchem-193	160	31	with	with	ADP
eurjchem-193	160	32	the	the	DET
eurjchem-193	160	33	observed	observe	VERB
eurjchem-193	160	34	data	datum	NOUN
eurjchem-193	160	35	given	give	VERB
eurjchem-193	160	36	in	in	ADP
eurjchem-193	160	37	the	the	DET
eurjchem-193	160	38	experimental	experimental	ADJ
eurjchem-193	160	39	part	part	NOUN
eurjchem-193	160	40	.	.	PUNCT
eurjchem-193	161	1	furthermore	furthermore	ADV
eurjchem-193	161	2	,	,	PUNCT
eurjchem-193	161	3	the	the	DET
eurjchem-193	161	4	negative	negative	ADJ
eurjchem-193	161	5	field	field	NOUN
eurjchem-193	161	6	of	of	ADP
eurjchem-193	161	7	the	the	DET
eurjchem-193	161	8	carbonyl	carbonyl	NOUN
eurjchem-193	161	9	oxygen	oxygen	NOUN
eurjchem-193	161	10	suffers	suffer	VERB
eurjchem-193	161	11	from	from	ADP
eurjchem-193	161	12	the	the	DET
eurjchem-193	161	13	repulsive	repulsive	ADJ
eurjchem-193	161	14	forces	force	NOUN
eurjchem-193	161	15	with	with	ADP
eurjchem-193	161	16	the	the	DET
eurjchem-193	161	17	π‐cloud	π‐cloud	PUNCT
eurjchem-193	161	18	of	of	ADP
eurjchem-193	161	19	the	the	DET
eurjchem-193	161	20	aromatic	aromatic	ADJ
eurjchem-193	161	21	ring	ring	NOUN
eurjchem-193	161	22	in	in	ADP
eurjchem-193	161	23	case	case	NOUN
eurjchem-193	161	24	of	of	ADP
eurjchem-193	161	25	e‐configuration	e‐configuration	PUNCT
eurjchem-193	161	26	and	and	CCONJ
eurjchem-193	161	27	hence	hence	ADV
eurjchem-193	161	28	the	the	DET
eurjchem-193	161	29	compound	compound	NOUN
eurjchem-193	161	30	favours	favour	VERB
eurjchem-193	161	31	the	the	DET
eurjchem-193	161	32	formation	formation	NOUN
eurjchem-193	161	33	of	of	ADP
eurjchem-193	161	34	the	the	DET
eurjchem-193	161	35	structure	structure	NOUN
eurjchem-193	161	36	shown	show	VERB
eurjchem-193	161	37	in	in	ADP
eurjchem-193	161	38	scheme	scheme	NOUN
eurjchem-193	161	39	1	1	NUM
eurjchem-193	161	40	.	.	PUNCT
eurjchem-193	162	1	the	the	DET
eurjchem-193	162	2	formation	formation	NOUN
eurjchem-193	162	3	of	of	ADP
eurjchem-193	162	4	3	3	NUM
eurjchem-193	162	5	was	be	AUX
eurjchem-193	162	6	assumed	assume	VERB
eurjchem-193	162	7	to	to	PART
eurjchem-193	162	8	proceed	proceed	VERB
eurjchem-193	162	9	via	via	ADP
eurjchem-193	162	10	nucleophilic	nucleophilic	ADJ
eurjchem-193	162	11	addition	addition	NOUN
eurjchem-193	162	12	of	of	ADP
eurjchem-193	162	13	the	the	DET
eurjchem-193	162	14	thiazolidinyl‐c‐5	thiazolidinyl‐c‐5	NOUN
eurjchem-193	162	15	to	to	ADP
eurjchem-193	162	16	the	the	PRON
eurjchem-193	162	17	β‐carbon	β‐carbon	PUNCT
eurjchem-193	162	18	of	of	ADP
eurjchem-193	162	19	the	the	DET
eurjchem-193	162	20	activated	activate	VERB
eurjchem-193	162	21	double	double	ADJ
eurjchem-193	162	22	bond	bond	NOUN
eurjchem-193	162	23	of	of	ADP
eurjchem-193	162	24	1	1	NUM
eurjchem-193	162	25	forming	form	VERB
eurjchem-193	162	26	the	the	DET
eurjchem-193	162	27	1:1	1:1	NUM
eurjchem-193	162	28	adduct	adduct	NOUN
eurjchem-193	162	29	followed	follow	VERB
eurjchem-193	162	30	by	by	ADP
eurjchem-193	162	31	removal	removal	NOUN
eurjchem-193	162	32	of	of	ADP
eurjchem-193	162	33	malononitrile	malononitrile	NOUN
eurjchem-193	162	34	or	or	CCONJ
eurjchem-193	162	35	ethylcyanoacetate	ethylcyanoacetate	VERB
eurjchem-193	162	36	molecule	molecule	NOUN
eurjchem-193	162	37	(	(	PUNCT
eurjchem-193	162	38	scheme	scheme	NOUN
eurjchem-193	162	39	2	2	NUM
eurjchem-193	162	40	)	)	PUNCT
eurjchem-193	162	41	.	.	PUNCT
eurjchem-193	163	1	when	when	SCONJ
eurjchem-193	163	2	(	(	PUNCT
eurjchem-193	163	3	z)‐2‐imino‐5‐(3,4,5‐trimethoxybenzylidene)‐thia‐	z)‐2‐imino‐5‐(3,4,5‐trimethoxybenzylidene)‐thia‐	NUM
eurjchem-193	163	4	zolidin‐4(h)‐one	zolidin‐4(h)‐one	NUM
eurjchem-193	163	5	(	(	PUNCT
eurjchem-193	163	6	3	3	NUM
eurjchem-193	163	7	)	)	PUNCT
eurjchem-193	163	8	was	be	AUX
eurjchem-193	163	9	subjected	subject	VERB
eurjchem-193	163	10	to	to	PART
eurjchem-193	163	11	react	react	VERB
eurjchem-193	163	12	with	with	ADP
eurjchem-193	163	13	benzyl	benzyl	NOUN
eurjchem-193	163	14	amine	amine	NOUN
eurjchem-193	163	15	in	in	ADP
eurjchem-193	163	16	refluxing	refluxing	NOUN
eurjchem-193	163	17	ethanol	ethanol	NOUN
eurjchem-193	163	18	,	,	PUNCT
eurjchem-193	163	19	h2s	h2s	NOUN
eurjchem-193	163	20	released	release	VERB
eurjchem-193	163	21	during	during	ADP
eurjchem-193	163	22	the	the	DET
eurjchem-193	163	23	reaction	reaction	NOUN
eurjchem-193	163	24	period	period	NOUN
eurjchem-193	163	25	and	and	CCONJ
eurjchem-193	163	26	a	a	DET
eurjchem-193	163	27	sulfur	sulfur	NOUN
eurjchem-193	163	28	free	free	ADJ
eurjchem-193	163	29	compound	compound	NOUN
eurjchem-193	163	30	with	with	ADP
eurjchem-193	163	31	molecular	molecular	ADJ
eurjchem-193	163	32	formula	formula	NOUN
eurjchem-193	163	33	c27h25n3o4	c27h25n3o4	VERB
eurjchem-193	163	34	is	be	AUX
eurjchem-193	163	35	produced	produce	VERB
eurjchem-193	163	36	which	which	PRON
eurjchem-193	163	37	indicates	indicate	VERB
eurjchem-193	163	38	the	the	DET
eurjchem-193	163	39	incorporation	incorporation	NOUN
eurjchem-193	163	40	of	of	ADP
eurjchem-193	163	41	two	two	NUM
eurjchem-193	163	42	molecules	molecule	NOUN
eurjchem-193	163	43	of	of	ADP
eurjchem-193	163	44	benzyl	benzyl	NOUN
eurjchem-193	163	45	amine	amine	NOUN
eurjchem-193	163	46	.	.	PUNCT
eurjchem-193	164	1	this	this	DET
eurjchem-193	164	2	compound	compound	NOUN
eurjchem-193	164	3	was	be	AUX
eurjchem-193	164	4	identified	identify	VERB
eurjchem-193	164	5	to	to	PART
eurjchem-193	164	6	be	be	AUX
eurjchem-193	164	7	(	(	PUNCT
eurjchem-193	164	8	2e	2e	NUM
eurjchem-193	164	9	,	,	PUNCT
eurjchem-193	164	10	5z)‐	5z)‐	NUM
eurjchem-193	164	11	1‐benzyl‐2‐benzylimino‐5‐(3,4,5‐trimethoxy	1‐benzyl‐2‐benzylimino‐5‐(3,4,5‐trimethoxy	NUM
eurjchem-193	164	12	benzylidene)‐	benzylidene)‐	PROPN
eurjchem-193	164	13	imidazolidin‐4(h)one	imidazolidin‐4(h)one	NOUN
eurjchem-193	164	14	(	(	PUNCT
eurjchem-193	164	15	4	4	NUM
eurjchem-193	164	16	)	)	PUNCT
eurjchem-193	164	17	from	from	ADP
eurjchem-193	164	18	microanalytical	microanalytical	ADJ
eurjchem-193	164	19	data	datum	NOUN
eurjchem-193	164	20	and	and	CCONJ
eurjchem-193	164	21	spectroscopic	spectroscopic	ADJ
eurjchem-193	164	22	analysis	analysis	NOUN
eurjchem-193	164	23	(	(	PUNCT
eurjchem-193	164	24	scheme	scheme	NOUN
eurjchem-193	164	25	3	3	NUM
eurjchem-193	164	26	)	)	PUNCT
eurjchem-193	164	27	.	.	PUNCT
eurjchem-193	165	1	differing	differ	VERB
eurjchem-193	165	2	accounts	account	NOUN
eurjchem-193	165	3	dealing	deal	VERB
eurjchem-193	165	4	with	with	ADP
eurjchem-193	165	5	action	action	NOUN
eurjchem-193	165	6	of	of	ADP
eurjchem-193	165	7	hydrazine	hydrazine	NOUN
eurjchem-193	165	8	hydrate	hydrate	NOUN
eurjchem-193	165	9	on	on	ADP
eurjchem-193	165	10	thiazolidinone	thiazolidinone	NOUN
eurjchem-193	165	11	derivatives	derivative	NOUN
eurjchem-193	165	12	were	be	AUX
eurjchem-193	165	13	reported	report	VERB
eurjchem-193	165	14	[	[	X
eurjchem-193	165	15	11‐13	11‐13	NUM
eurjchem-193	165	16	]	]	PUNCT
eurjchem-193	165	17	.	.	PUNCT
eurjchem-193	166	1	omer	omer	PROPN
eurjchem-193	166	2	and	and	CCONJ
eurjchem-193	166	3	rauof	rauof	VERB
eurjchem-193	166	4	et	et	PROPN
eurjchem-193	166	5	al	al	PROPN
eurjchem-193	166	6	.	.	PUNCT
eurjchem-193	167	1	[	[	X
eurjchem-193	167	2	12	12	NUM
eurjchem-193	167	3	]	]	PUNCT
eurjchem-193	167	4	reported	report	VERB
eurjchem-193	167	5	the	the	DET
eurjchem-193	167	6	cleavage	cleavage	NOUN
eurjchem-193	167	7	of	of	ADP
eurjchem-193	167	8	5‐arylmethylene‐2,4‐	5‐arylmethylene‐2,4‐	NUM
eurjchem-193	167	9	dioxo‐1,3‐thiazolidines	dioxo‐1,3‐thiazolidine	NOUN
eurjchem-193	167	10	with	with	ADP
eurjchem-193	167	11	hydrazines	hydrazine	NOUN
eurjchem-193	167	12	and	and	CCONJ
eurjchem-193	167	13	afforded	afford	VERB
eurjchem-193	167	14	the	the	DET
eurjchem-193	167	15	respective	respective	ADJ
eurjchem-193	167	16	triazinones	triazinone	NOUN
eurjchem-193	167	17	.	.	PUNCT
eurjchem-193	168	1	here	here	ADV
eurjchem-193	168	2	in	in	ADP
eurjchem-193	168	3	,	,	PUNCT
eurjchem-193	168	4	hydrazinolysis	hydrazinolysis	NOUN
eurjchem-193	168	5	of	of	ADP
eurjchem-193	168	6	compound	compound	NOUN
eurjchem-193	168	7	3	3	NUM
eurjchem-193	168	8	in	in	ADP
eurjchem-193	168	9	refluxing	refluxing	NOUN
eurjchem-193	168	10	n‐butanol	n‐butanol	VERB
eurjchem-193	168	11	afforded	afford	VERB
eurjchem-193	168	12	the	the	DET
eurjchem-193	168	13	dimeric	dimeric	ADJ
eurjchem-193	168	14	product	product	NOUN
eurjchem-193	168	15	5	5	NUM
eurjchem-193	168	16	(	(	PUNCT
eurjchem-193	168	17	scheme	scheme	NOUN
eurjchem-193	168	18	3	3	NUM
eurjchem-193	168	19	)	)	PUNCT
eurjchem-193	168	20	.	.	PUNCT
eurjchem-193	169	1	several	several	ADJ
eurjchem-193	169	2	authors	author	NOUN
eurjchem-193	169	3	reported	report	VERB
eurjchem-193	169	4	the	the	DET
eurjchem-193	169	5	formation	formation	NOUN
eurjchem-193	169	6	of	of	ADP
eurjchem-193	169	7	piperidino	piperidino	NOUN
eurjchem-193	169	8	and	and	CCONJ
eurjchem-193	169	9	morpholino	morpholino	PROPN
eurjchem-193	169	10	salts	salt	NOUN
eurjchem-193	169	11	of	of	ADP
eurjchem-193	169	12	5‐arylmethylene‐4‐oxo‐2‐thioxo‐thiazo‐	5‐arylmethylene‐4‐oxo‐2‐thioxo‐thiazo‐	NUM
eurjchem-193	169	13	lidines	lidine	NOUN
eurjchem-193	169	14	by	by	ADP
eurjchem-193	169	15	reacting	react	VERB
eurjchem-193	169	16	3h‐thiazolinones	3h‐thiazolinone	NOUN
eurjchem-193	169	17	with	with	ADP
eurjchem-193	169	18	the	the	DET
eurjchem-193	169	19	required	require	VERB
eurjchem-193	169	20	secondary	secondary	ADJ
eurjchem-193	169	21	amine	amine	NOUN
eurjchem-193	169	22	in	in	ADP
eurjchem-193	169	23	acetone	acetone	NOUN
eurjchem-193	169	24	or	or	CCONJ
eurjchem-193	169	25	methyl	methyl	NOUN
eurjchem-193	169	26	acetate	acetate	NOUN
eurjchem-193	169	27	solution	solution	NOUN
eurjchem-193	169	28	[	[	X
eurjchem-193	169	29	11,12	11,12	NOUN
eurjchem-193	169	30	]	]	PUNCT
eurjchem-193	169	31	.	.	PUNCT
eurjchem-193	170	1	treatment	treatment	NOUN
eurjchem-193	170	2	of	of	ADP
eurjchem-193	170	3	(	(	PUNCT
eurjchem-193	170	4	z)‐2‐imino‐5‐(3,4,5‐trimethoxybenzylidene)‐	z)‐2‐imino‐5‐(3,4,5‐trimethoxybenzylidene)‐	NOUN
eurjchem-193	170	5	thiazolidin‐4‐one	thiazolidin‐4‐one	X
eurjchem-193	170	6	(	(	PUNCT
eurjchem-193	170	7	3	3	X
eurjchem-193	170	8	)	)	PUNCT
eurjchem-193	170	9	with	with	ADP
eurjchem-193	170	10	piperidine	piperidine	NOUN
eurjchem-193	170	11	afforded	afford	VERB
eurjchem-193	170	12	the	the	DET
eurjchem-193	170	13	compound	compound	NOUN
eurjchem-193	170	14	6	6	NUM
eurjchem-193	170	15	which	which	PRON
eurjchem-193	170	16	assigned	assign	VERB
eurjchem-193	170	17	as	as	ADP
eurjchem-193	170	18	(	(	PUNCT
eurjchem-193	170	19	z)‐2‐(piperidin‐1‐yl)‐5‐(3,4,5‐trimethoxy	z)‐2‐(piperidin‐1‐yl)‐5‐(3,4,5‐trimethoxy	INTJ
eurjchem-193	170	20	benzylidene)thiazol‐4(5h)one	benzylidene)thiazol‐4(5h)one	PROPN
eurjchem-193	170	21	(	(	PUNCT
eurjchem-193	170	22	c.f	c.f	PROPN
eurjchem-193	170	23	.	.	PROPN
eurjchem-193	170	24	exp	exp	PROPN
eurjchem-193	170	25	.	.	PUNCT
eurjchem-193	170	26	)	)	PUNCT
eurjchem-193	170	27	.	.	PUNCT
eurjchem-193	171	1	the	the	DET
eurjchem-193	171	2	reaction	reaction	NOUN
eurjchem-193	171	3	of	of	ADP
eurjchem-193	171	4	grignard	grignard	ADJ
eurjchem-193	171	5	reagents	reagent	NOUN
eurjchem-193	171	6	with	with	ADP
eurjchem-193	171	7	various	various	ADJ
eurjchem-193	171	8	5‐arylidene‐	5‐arylidene‐	NUM
eurjchem-193	171	9	1,3‐thiazolidines	1,3‐thiazolidine	NOUN
eurjchem-193	171	10	and	and	CCONJ
eurjchem-193	171	11	its	its	PRON
eurjchem-193	171	12	piperidino	piperidino	NOUN
eurjchem-193	171	13	salts	salt	NOUN
eurjchem-193	171	14	have	have	AUX
eurjchem-193	171	15	been	be	AUX
eurjchem-193	171	16	reported	report	VERB
eurjchem-193	171	17	[	[	X
eurjchem-193	171	18	14	14	NUM
eurjchem-193	171	19	]	]	PUNCT
eurjchem-193	171	20	.	.	PUNCT
eurjchem-193	172	1	actually	actually	ADV
eurjchem-193	172	2	,	,	PUNCT
eurjchem-193	172	3	the	the	DET
eurjchem-193	172	4	majority	majority	NOUN
eurjchem-193	172	5	of	of	ADP
eurjchem-193	172	6	the	the	DET
eurjchem-193	172	7	products	product	NOUN
eurjchem-193	172	8	resulted	result	VERB
eurjchem-193	172	9	from	from	ADP
eurjchem-193	172	10	the	the	DET
eurjchem-193	172	11	action	action	NOUN
eurjchem-193	172	12	of	of	ADP
eurjchem-193	172	13	cyclohexyl	cyclohexyl	PROPN
eurjchem-193	172	14	magnesium	magnesium	PROPN
eurjchem-193	172	15	bromide	bromide	NOUN
eurjchem-193	172	16	and	and	CCONJ
eurjchem-193	172	17	phenyl	phenyl	NOUN
eurjchem-193	172	18	magnesium	magnesium	NOUN
eurjchem-193	172	19	bromide	bromide	NOUN
eurjchem-193	172	20	on	on	ADP
eurjchem-193	172	21	6	6	NUM
eurjchem-193	172	22	represents	represent	VERB
eurjchem-193	172	23	some	some	PRON
eurjchem-193	172	24	of	of	ADP
eurjchem-193	172	25	the	the	DET
eurjchem-193	172	26	mentioned	mention	VERB
eurjchem-193	172	27	routes	route	NOUN
eurjchem-193	172	28	(	(	PUNCT
eurjchem-193	172	29	1,2‐addition	1,2‐addition	NOUN
eurjchem-193	172	30	at	at	ADP
eurjchem-193	172	31	c	c	NOUN
eurjchem-193	172	32	=	=	SYM
eurjchem-193	172	33	n	n	X
eurjchem-193	172	34	,	,	PUNCT
eurjchem-193	172	35	c	c	PROPN
eurjchem-193	172	36	=	=	X
eurjchem-193	172	37	o	o	NOUN
eurjchem-193	172	38	and	and	CCONJ
eurjchem-193	172	39	1,4‐addition	1,4‐addition	NUM
eurjchem-193	172	40	to	to	ADP
eurjchem-193	172	41	c	c	X
eurjchem-193	172	42	=	=	X
eurjchem-193	172	43	c‐c	c‐c	X
eurjchem-193	172	44	=	=	NOUN
eurjchem-193	172	45	o	o	PROPN
eurjchem-193	172	46	and	and	CCONJ
eurjchem-193	172	47	c	c	X
eurjchem-193	172	48	=	=	ADJ
eurjchem-193	172	49	c‐c	c‐c	NOUN
eurjchem-193	172	50	=	=	NOUN
eurjchem-193	172	51	n	n	NUM
eurjchem-193	172	52	)	)	PUNCT
eurjchem-193	172	53	.	.	PUNCT
eurjchem-193	173	1	thus	thus	ADV
eurjchem-193	173	2	,	,	PUNCT
eurjchem-193	173	3	the	the	DET
eurjchem-193	173	4	reaction	reaction	NOUN
eurjchem-193	173	5	of	of	ADP
eurjchem-193	173	6	6	6	NUM
eurjchem-193	173	7	with	with	ADP
eurjchem-193	173	8	phenyl	phenyl	NOUN
eurjchem-193	173	9	magnesium	magnesium	NOUN
eurjchem-193	173	10	bromide	bromide	NOUN
eurjchem-193	173	11	in	in	ADP
eurjchem-193	173	12	refluxing	refluxing	NOUN
eurjchem-193	173	13	ether‐anhydrous	ether‐anhydrous	ADJ
eurjchem-193	173	14	benzene	benzene	NOUN
eurjchem-193	173	15	mixture	mixture	NOUN
eurjchem-193	173	16	afforded	afford	VERB
eurjchem-193	173	17	the	the	DET
eurjchem-193	173	18	adduct	adduct	NOUN
eurjchem-193	173	19	7	7	NUM
eurjchem-193	173	20	.	.	PUNCT
eurjchem-193	174	1	the	the	DET
eurjchem-193	174	2	structure	structure	NOUN
eurjchem-193	174	3	of	of	ADP
eurjchem-193	174	4	7	7	NUM
eurjchem-193	174	5	was	be	AUX
eurjchem-193	174	6	evidenced	evidence	VERB
eurjchem-193	174	7	by	by	ADP
eurjchem-193	174	8	analytical	analytical	ADJ
eurjchem-193	174	9	data	datum	NOUN
eurjchem-193	174	10	which	which	PRON
eurjchem-193	174	11	infers	infer	VERB
eurjchem-193	174	12	the	the	DET
eurjchem-193	174	13	incorporation	incorporation	NOUN
eurjchem-193	174	14	of	of	ADP
eurjchem-193	174	15	two	two	NUM
eurjchem-193	174	16	molar	molar	ADJ
eurjchem-193	174	17	proportions	proportion	NOUN
eurjchem-193	174	18	of	of	ADP
eurjchem-193	174	19	the	the	DET
eurjchem-193	174	20	grignard	grignard	ADJ
eurjchem-193	174	21	reagent	reagent	NOUN
eurjchem-193	174	22	.	.	PUNCT
eurjchem-193	175	1	the	the	DET
eurjchem-193	175	2	transformation	transformation	NOUN
eurjchem-193	175	3	of	of	ADP
eurjchem-193	175	4	6	6	NUM
eurjchem-193	175	5	to	to	PART
eurjchem-193	175	6	7	7	NUM
eurjchem-193	175	7	was	be	AUX
eurjchem-193	175	8	represented	represent	VERB
eurjchem-193	175	9	in	in	ADP
eurjchem-193	175	10	scheme	scheme	NOUN
eurjchem-193	175	11	4	4	NUM
eurjchem-193	175	12	,	,	PUNCT
eurjchem-193	175	13	it	it	PRON
eurjchem-193	175	14	is	be	AUX
eurjchem-193	175	15	supported	support	VERB
eurjchem-193	175	16	that	that	SCONJ
eurjchem-193	175	17	the	the	DET
eurjchem-193	175	18	reaction	reaction	NOUN
eurjchem-193	175	19	has	have	AUX
eurjchem-193	175	20	occurred	occur	VERB
eurjchem-193	175	21	either	either	CCONJ
eurjchem-193	175	22	through	through	ADP
eurjchem-193	175	23	1,2‐addition	1,2‐addition	NOUN
eurjchem-193	175	24	to	to	ADP
eurjchem-193	175	25	c	c	NOUN
eurjchem-193	175	26	=	=	SYM
eurjchem-193	175	27	n	n	DET
eurjchem-193	175	28	group	group	NOUN
eurjchem-193	175	29	of	of	ADP
eurjchem-193	175	30	the	the	DET
eurjchem-193	175	31	thiazolidine	thiazolidine	PROPN
eurjchem-193	175	32	ring	ring	NOUN
eurjchem-193	175	33	,	,	PUNCT
eurjchem-193	175	34	or	or	CCONJ
eurjchem-193	175	35	through	through	ADP
eurjchem-193	175	36	the	the	DET
eurjchem-193	175	37	transition	transition	NOUN
eurjchem-193	175	38	state	state	NOUN
eurjchem-193	176	1	[	[	X
eurjchem-193	176	2	a	a	X
eurjchem-193	176	3	]	]	X
eurjchem-193	176	4	which	which	PRON
eurjchem-193	176	5	resulted	result	VERB
eurjchem-193	176	6	from	from	ADP
eurjchem-193	176	7	the	the	DET
eurjchem-193	176	8	1,4‐addition	1,4‐addition	NUM
eurjchem-193	176	9	to	to	ADP
eurjchem-193	176	10	c	c	X
eurjchem-193	176	11	=	=	X
eurjchem-193	176	12	c‐c	c‐c	PROPN
eurjchem-193	176	13	=	=	NOUN
eurjchem-193	176	14	o	o	NOUN
eurjchem-193	176	15	ring	ring	NOUN
eurjchem-193	176	16	system	system	NOUN
eurjchem-193	176	17	followed	follow	VERB
eurjchem-193	176	18	by	by	ADP
eurjchem-193	176	19	rearrangement	rearrangement	NOUN
eurjchem-193	176	20	(	(	PUNCT
eurjchem-193	176	21	scheme	scheme	NOUN
eurjchem-193	176	22	4	4	NUM
eurjchem-193	176	23	)	)	PUNCT
eurjchem-193	176	24	.	.	PUNCT
eurjchem-193	177	1	cyclohexyl	cyclohexyl	PROPN
eurjchem-193	177	2	magnesium	magnesium	NOUN
eurjchem-193	177	3	bromide	bromide	NOUN
eurjchem-193	177	4	attacks	attack	NOUN
eurjchem-193	177	5	2‐piperidino	2‐piperidino	NUM
eurjchem-193	177	6	derivative	derivative	ADJ
eurjchem-193	177	7	6	6	NUM
eurjchem-193	177	8	in	in	ADP
eurjchem-193	177	9	refluxing	refluxing	NOUN
eurjchem-193	177	10	ether‐anhydrous	ether‐anhydrous	ADJ
eurjchem-193	177	11	benzene	benzene	NOUN
eurjchem-193	177	12	mixture	mixture	NOUN
eurjchem-193	177	13	through	through	ADP
eurjchem-193	177	14	1,2‐addition	1,2‐addition	NOUN
eurjchem-193	177	15	at	at	ADP
eurjchem-193	177	16	c	c	NOUN
eurjchem-193	177	17	=	=	NOUN
eurjchem-193	177	18	n	n	PART
eurjchem-193	177	19	to	to	PART
eurjchem-193	177	20	give	give	VERB
eurjchem-193	177	21	(	(	PUNCT
eurjchem-193	177	22	z)‐2‐cyclohexyl‐2‐	z)‐2‐cyclohexyl‐2‐	X
eurjchem-193	177	23	(	(	PUNCT
eurjchem-193	177	24	piperidin‐1‐yl)‐5‐(3,4,5‐trimethoxybenzylidene)‐thiazolidin‐	piperidin‐1‐yl)‐5‐(3,4,5‐trimethoxybenzylidene)‐thiazolidin‐	NOUN
eurjchem-193	177	25	4‐one	4‐one	NUM
eurjchem-193	177	26	(	(	PUNCT
eurjchem-193	177	27	8)	8)	NUM
eurjchem-193	177	28	.	.	PUNCT
eurjchem-193	178	1	the	the	DET
eurjchem-193	178	2	structure	structure	NOUN
eurjchem-193	178	3	of	of	ADP
eurjchem-193	178	4	8	8	NUM
eurjchem-193	178	5	is	be	AUX
eurjchem-193	178	6	substantiated	substantiate	VERB
eurjchem-193	178	7	by	by	ADP
eurjchem-193	178	8	microanalysis	microanalysis	NOUN
eurjchem-193	178	9	which	which	PRON
eurjchem-193	178	10	infers	infer	VERB
eurjchem-193	178	11	the	the	DET
eurjchem-193	178	12	addition	addition	NOUN
eurjchem-193	178	13	of	of	ADP
eurjchem-193	178	14	one	one	NUM
eurjchem-193	178	15	molecule	molecule	NOUN
eurjchem-193	178	16	of	of	ADP
eurjchem-193	178	17	cyclohexane	cyclohexane	NOUN
eurjchem-193	178	18	and	and	CCONJ
eurjchem-193	178	19	confirmed	confirm	VERB
eurjchem-193	178	20	by	by	ADP
eurjchem-193	178	21	ir	ir	PROPN
eurjchem-193	178	22	spectrum	spectrum	NOUN
eurjchem-193	178	23	which	which	PRON
eurjchem-193	178	24	exhibits	exhibit	VERB
eurjchem-193	178	25	the	the	DET
eurjchem-193	178	26	strong	strong	ADJ
eurjchem-193	178	27	absorption	absorption	NOUN
eurjchem-193	178	28	bands	band	NOUN
eurjchem-193	178	29	characteristic	characteristic	ADJ
eurjchem-193	178	30	for	for	ADP
eurjchem-193	178	31	nh	nh	PROPN
eurjchem-193	178	32	(	(	PUNCT
eurjchem-193	178	33	br	br	PROPN
eurjchem-193	178	34	.	.	PUNCT
eurjchem-193	178	35	)	)	PUNCT
eurjchem-193	178	36	,	,	PUNCT
eurjchem-193	178	37	c‐h	c‐h	PROPN
eurjchem-193	178	38	(	(	PUNCT
eurjchem-193	178	39	str	str	NOUN
eurjchem-193	178	40	.	.	PUNCT
eurjchem-193	178	41	)	)	PUNCT
eurjchem-193	178	42	,	,	PUNCT
eurjchem-193	178	43	and	and	CCONJ
eurjchem-193	178	44	c	c	X
eurjchem-193	178	45	=	=	NOUN
eurjchem-193	178	46	o	o	X
eurjchem-193	178	47	of	of	ADP
eurjchem-193	178	48	thiazolidine	thiazolidine	PROPN
eurjchem-193	178	49	ring	ring	NOUN
eurjchem-193	178	50	and	and	CCONJ
eurjchem-193	178	51	was	be	AUX
eurjchem-193	178	52	rigidly	rigidly	ADV
eurjchem-193	178	53	established	establish	VERB
eurjchem-193	178	54	by	by	ADP
eurjchem-193	178	55	mass	mass	NOUN
eurjchem-193	178	56	spectrum	spectrum	NOUN
eurjchem-193	178	57	which	which	PRON
eurjchem-193	178	58	shows	show	VERB
eurjchem-193	178	59	fragmentation	fragmentation	NOUN
eurjchem-193	178	60	pattern	pattern	NOUN
eurjchem-193	178	61	consistent	consistent	ADJ
eurjchem-193	178	62	with	with	ADP
eurjchem-193	178	63	the	the	DET
eurjchem-193	178	64	assigned	assign	VERB
eurjchem-193	178	65	structure	structure	NOUN
eurjchem-193	178	66	8	8	NUM
eurjchem-193	178	67	(	(	PUNCT
eurjchem-193	178	68	c.f	c.f	PROPN
eurjchem-193	178	69	.	.	PROPN
eurjchem-193	178	70	exp	exp	PROPN
eurjchem-193	178	71	.	.	PUNCT
eurjchem-193	178	72	)	)	PUNCT
eurjchem-193	178	73	.	.	PUNCT
eurjchem-193	179	1	the	the	DET
eurjchem-193	179	2	carbanion	carbanion	NOUN
eurjchem-193	179	3	which	which	PRON
eurjchem-193	179	4	derived	derive	VERB
eurjchem-193	179	5	from	from	ADP
eurjchem-193	179	6	ethyl	ethyl	PROPN
eurjchem-193	179	7	cyanoacetate	cyanoacetate	NOUN
eurjchem-193	179	8	in	in	ADP
eurjchem-193	179	9	anhydrous	anhydrous	ADJ
eurjchem-193	179	10	benzene	benzene	NOUN
eurjchem-193	179	11	upon	upon	SCONJ
eurjchem-193	179	12	treating	treat	VERB
eurjchem-193	179	13	with	with	ADP
eurjchem-193	179	14	sodium	sodium	NOUN
eurjchem-193	179	15	hydride	hydride	NOUN
eurjchem-193	179	16	reacted	react	VERB
eurjchem-193	179	17	with	with	ADP
eurjchem-193	179	18	compound	compound	NOUN
eurjchem-193	179	19	6	6	NUM
eurjchem-193	179	20	to	to	PART
eurjchem-193	179	21	afford	afford	VERB
eurjchem-193	179	22	orange	orange	PROPN
eurjchem-193	179	23	solid	solid	ADJ
eurjchem-193	179	24	product	product	NOUN
eurjchem-193	179	25	from	from	ADP
eurjchem-193	179	26	which	which	PRON
eurjchem-193	179	27	it	it	PRON
eurjchem-193	179	28	is	be	AUX
eurjchem-193	179	29	possible	possible	ADJ
eurjchem-193	179	30	to	to	PART
eurjchem-193	179	31	isolate	isolate	VERB
eurjchem-193	179	32	(	(	PUNCT
eurjchem-193	179	33	z)‐2‐	z)‐2‐	NUM
eurjchem-193	179	34	[	[	X
eurjchem-193	179	35	4‐oxo‐2‐(piperidin‐1‐yl)‐5‐(3,4,5‐trimethoxybenzylidene)‐	4‐oxo‐2‐(piperidin‐1‐yl)‐5‐(3,4,5‐trimethoxybenzylidene)‐	NUM
eurjchem-193	179	36	thiazolidin‐2‐yl]malonic	thiazolidin‐2‐yl]malonic	NOUN
eurjchem-193	179	37	acid	acid	NOUN
eurjchem-193	179	38	(	(	PUNCT
eurjchem-193	179	39	9	9	NUM
eurjchem-193	179	40	)	)	PUNCT
eurjchem-193	179	41	.	.	PUNCT
eurjchem-193	180	1	madmoud	madmoud	NOUN
eurjchem-193	180	2	et	et	PROPN
eurjchem-193	180	3	al	al	PROPN
eurjchem-193	180	4	.	.	PUNCT
eurjchem-193	180	5	/	/	SYM
eurjchem-193	180	6	european	european	PROPN
eurjchem-193	180	7	journal	journal	PROPN
eurjchem-193	180	8	of	of	ADP
eurjchem-193	180	9	chemistry	chemistry	NOUN
eurjchem-193	180	10	2	2	NUM
eurjchem-193	180	11	(	(	PUNCT
eurjchem-193	180	12	4	4	NUM
eurjchem-193	180	13	)	)	PUNCT
eurjchem-193	180	14	(	(	PUNCT
eurjchem-193	180	15	2011	2011	NUM
eurjchem-193	180	16	)	)	PUNCT
eurjchem-193	181	1	475‐479	475‐479	NUM
eurjchem-193	181	2	479	479	NUM
eurjchem-193	182	1	n	n	NOUN
eurjchem-193	182	2	s	s	X
eurjchem-193	182	3	o	o	X
eurjchem-193	182	4	har	har	PROPN
eurjchem-193	182	5	n	n	CCONJ
eurjchem-193	182	6	(	(	PUNCT
eurjchem-193	182	7	6	6	NUM
eurjchem-193	182	8	)	)	PUNCT
eurjchem-193	182	9	n	n	PRON
eurjchem-193	182	10	s	s	PART
eurjchem-193	182	11	o	o	X
eurjchem-193	182	12	har	har	PROPN
eurjchem-193	183	1	n	n	CCONJ
eurjchem-193	183	2	k	k	NOUN
eurjchem-193	184	1	oh	oh	INTJ
eurjchem-193	184	2	oh	oh	INTJ
eurjchem-193	185	1	n	n	PRON
eurjchem-193	185	2	s	s	X
eurjchem-193	185	3	o	o	X
eurjchem-193	185	4	har	har	NOUN
eurjchem-193	186	1	oh	oh	INTJ
eurjchem-193	186	2	n	n	CCONJ
eurjchem-193	186	3	k	k	PROPN
eurjchem-193	186	4	s	s	X
eurjchem-193	186	5	o	o	X
eurjchem-193	186	6	har	har	X
eurjchem-193	186	7	o	o	NOUN
eurjchem-193	187	1	+	+	CCONJ
eurjchem-193	187	2	c5h11n	c5h11n	ADJ
eurjchem-193	187	3	(	(	PUNCT
eurjchem-193	187	4	10	10	NUM
eurjchem-193	187	5	)	)	PUNCT
eurjchem-193	187	6	c5h10n	c5h10n	PROPN
eurjchem-193	187	7	k	k	PROPN
eurjchem-193	187	8	scheme	scheme	PROPN
eurjchem-193	187	9	5	5	NUM
eurjchem-193	187	10	conversion	conversion	NOUN
eurjchem-193	187	11	of	of	ADP
eurjchem-193	187	12	6	6	NUM
eurjchem-193	187	13	into	into	ADP
eurjchem-193	187	14	the	the	DET
eurjchem-193	187	15	potassium	potassium	NOUN
eurjchem-193	187	16	salt	salt	NOUN
eurjchem-193	187	17	10	10	NUM
eurjchem-193	187	18	have	have	AUX
eurjchem-193	187	19	been	be	AUX
eurjchem-193	187	20	done	do	VERB
eurjchem-193	187	21	on	on	ADP
eurjchem-193	187	22	the	the	DET
eurjchem-193	187	23	basis	basis	NOUN
eurjchem-193	187	24	of	of	ADP
eurjchem-193	187	25	higher	high	ADJ
eurjchem-193	187	26	acidity	acidity	NOUN
eurjchem-193	187	27	of	of	ADP
eurjchem-193	187	28	3h‐compound	3h‐compound	NUM
eurjchem-193	187	29	following	follow	VERB
eurjchem-193	187	30	the	the	DET
eurjchem-193	187	31	reported	report	VERB
eurjchem-193	187	32	method	method	NOUN
eurjchem-193	187	33	[	[	X
eurjchem-193	187	34	12	12	NUM
eurjchem-193	187	35	]	]	PUNCT
eurjchem-193	187	36	by	by	ADP
eurjchem-193	187	37	treating	treat	VERB
eurjchem-193	187	38	6	6	NUM
eurjchem-193	187	39	with	with	ADP
eurjchem-193	187	40	ethanolic	ethanolic	ADJ
eurjchem-193	187	41	potassium	potassium	NOUN
eurjchem-193	187	42	hydroxide	hydroxide	NOUN
eurjchem-193	187	43	solution	solution	NOUN
eurjchem-193	187	44	.	.	PUNCT
eurjchem-193	188	1	formation	formation	NOUN
eurjchem-193	188	2	of	of	ADP
eurjchem-193	188	3	the	the	DET
eurjchem-193	188	4	salt	salt	NOUN
eurjchem-193	188	5	9	9	NUM
eurjchem-193	188	6	infers	infer	NOUN
eurjchem-193	188	7	that	that	PRON
eurjchem-193	188	8	the	the	DET
eurjchem-193	188	9	substituent	substituent	NOUN
eurjchem-193	188	10	at	at	ADP
eurjchem-193	188	11	the	the	DET
eurjchem-193	188	12	2‐position	2‐position	NUM
eurjchem-193	188	13	was	be	AUX
eurjchem-193	188	14	replaced	replace	VERB
eurjchem-193	188	15	through	through	ADP
eurjchem-193	188	16	the	the	DET
eurjchem-193	188	17	reaction	reaction	NOUN
eurjchem-193	188	18	(	(	PUNCT
eurjchem-193	188	19	scheme	scheme	NOUN
eurjchem-193	188	20	5	5	NUM
eurjchem-193	188	21	)	)	PUNCT
eurjchem-193	188	22	.	.	PUNCT
eurjchem-193	189	1	the	the	DET
eurjchem-193	189	2	ir	ir	PROPN
eurjchem-193	189	3	spectrum	spectrum	NOUN
eurjchem-193	189	4	of	of	ADP
eurjchem-193	189	5	10	10	NUM
eurjchem-193	189	6	show	show	NOUN
eurjchem-193	189	7	νc	νc	NOUN
eurjchem-193	189	8	=	=	NOUN
eurjchem-193	189	9	o	o	NOUN
eurjchem-193	189	10	at	at	ADP
eurjchem-193	189	11	relative	relative	ADJ
eurjchem-193	189	12	lower	low	ADJ
eurjchem-193	189	13	frequency	frequency	NOUN
eurjchem-193	189	14	(	(	PUNCT
eurjchem-193	189	15	1652	1652	NUM
eurjchem-193	189	16	cm‐1	cm‐1	NOUN
eurjchem-193	189	17	)	)	PUNCT
eurjchem-193	189	18	as	as	SCONJ
eurjchem-193	189	19	compared	compare	VERB
eurjchem-193	189	20	with	with	ADP
eurjchem-193	189	21	the	the	DET
eurjchem-193	189	22	extra	extra	ADJ
eurjchem-193	189	23	conjugation	conjugation	NOUN
eurjchem-193	189	24	performed	perform	VERB
eurjchem-193	189	25	by	by	ADP
eurjchem-193	189	26	the	the	DET
eurjchem-193	189	27	newly	newly	ADV
eurjchem-193	189	28	formed	form	VERB
eurjchem-193	189	29	negative	negative	ADJ
eurjchem-193	189	30	charge	charge	NOUN
eurjchem-193	189	31	.	.	PUNCT
eurjchem-193	190	1	furthermore	furthermore	ADV
eurjchem-193	190	2	,	,	PUNCT
eurjchem-193	190	3	1h	1h	NUM
eurjchem-193	190	4	nmr	nmr	NOUN
eurjchem-193	190	5	spectrum	spectrum	NOUN
eurjchem-193	190	6	of	of	ADP
eurjchem-193	190	7	10	10	NUM
eurjchem-193	190	8	show	show	NOUN
eurjchem-193	190	9	only	only	ADV
eurjchem-193	190	10	resonances	resonance	NOUN
eurjchem-193	190	11	of	of	ADP
eurjchem-193	190	12	aromatic	aromatic	ADJ
eurjchem-193	190	13	protons	proton	NOUN
eurjchem-193	190	14	(	(	PUNCT
eurjchem-193	190	15	2h	2h	NUM
eurjchem-193	190	16	)	)	PUNCT
eurjchem-193	190	17	at	at	ADP
eurjchem-193	190	18	δ	δ	PROPN
eurjchem-193	190	19	7.84	7.84	NUM
eurjchem-193	190	20	ppm	ppm	NOUN
eurjchem-193	190	21	together	together	ADV
eurjchem-193	190	22	with	with	ADP
eurjchem-193	190	23	olefinic	olefinic	ADJ
eurjchem-193	190	24	proton	proton	NOUN
eurjchem-193	190	25	at	at	ADP
eurjchem-193	190	26	δ	δ	PROPN
eurjchem-193	190	27	7.66	7.66	NUM
eurjchem-193	190	28	ppm	ppm	NOUN
eurjchem-193	190	29	,	,	PUNCT
eurjchem-193	190	30	and	and	CCONJ
eurjchem-193	190	31	two	two	NUM
eurjchem-193	190	32	singlets	singlet	NOUN
eurjchem-193	190	33	for	for	ADP
eurjchem-193	190	34	three	three	NUM
eurjchem-193	190	35	methoxy	methoxy	ADJ
eurjchem-193	190	36	protons	proton	NOUN
eurjchem-193	190	37	(	(	PUNCT
eurjchem-193	190	38	9h	9h	NUM
eurjchem-193	190	39	)	)	PUNCT
eurjchem-193	190	40	at	at	ADP
eurjchem-193	190	41	δ	δ	PROPN
eurjchem-193	190	42	(	(	PUNCT
eurjchem-193	190	43	ranged	range	VERB
eurjchem-193	190	44	from	from	ADP
eurjchem-193	190	45	3.9‐3.8	3.9‐3.8	NUM
eurjchem-193	190	46	ppm	ppm	NOUN
eurjchem-193	190	47	which	which	PRON
eurjchem-193	190	48	consistent	consistent	ADJ
eurjchem-193	190	49	with	with	ADP
eurjchem-193	190	50	the	the	DET
eurjchem-193	190	51	proposed	propose	VERB
eurjchem-193	190	52	structure	structure	NOUN
eurjchem-193	190	53	.	.	PUNCT
eurjchem-193	191	1	(	(	PUNCT
eurjchem-193	191	2	z)‐5‐(3,4,5‐trimethoxybenzylidene)‐3h‐thiazolidin‐	z)‐5‐(3,4,5‐trimethoxybenzylidene)‐3h‐thiazolidin‐	NUM
eurjchem-193	191	3	2,4‐dione	2,4‐dione	NUM
eurjchem-193	191	4	(	(	PUNCT
eurjchem-193	191	5	11	11	NUM
eurjchem-193	191	6	)	)	PUNCT
eurjchem-193	191	7	was	be	AUX
eurjchem-193	191	8	obtained	obtain	VERB
eurjchem-193	191	9	upon	upon	SCONJ
eurjchem-193	191	10	treating	treat	VERB
eurjchem-193	191	11	the	the	DET
eurjchem-193	191	12	potassium	potassium	NOUN
eurjchem-193	191	13	salt	salt	NOUN
eurjchem-193	191	14	10	10	NUM
eurjchem-193	191	15	with	with	ADP
eurjchem-193	191	16	dilute	dilute	VERB
eurjchem-193	191	17	acetic	acetic	ADJ
eurjchem-193	191	18	acid	acid	NOUN
eurjchem-193	191	19	.	.	PUNCT
eurjchem-193	192	1	alkylation	alkylation	NOUN
eurjchem-193	192	2	of	of	ADP
eurjchem-193	192	3	10	10	NUM
eurjchem-193	192	4	with	with	ADP
eurjchem-193	192	5	ethyl	ethyl	PROPN
eurjchem-193	192	6	chloroacetate	chloroacetate	NOUN
eurjchem-193	192	7	in	in	ADP
eurjchem-193	192	8	boiling	boiling	NOUN
eurjchem-193	192	9	ethanol	ethanol	NOUN
eurjchem-193	192	10	affords	afford	VERB
eurjchem-193	192	11	the	the	DET
eurjchem-193	192	12	n‐alkylation	n‐alkylation	NOUN
eurjchem-193	192	13	product	product	NOUN
eurjchem-193	192	14	(	(	PUNCT
eurjchem-193	192	15	z)ethyl‐2‐[2,4‐dioxo‐5‐(3,4,5‐	z)ethyl‐2‐[2,4‐dioxo‐5‐(3,4,5‐	PROPN
eurjchem-193	192	16	trimethoxybenzylidene)‐thiazolidin‐3‐yl]acetate	trimethoxybenzylidene)‐thiazolidin‐3‐yl]acetate	NOUN
eurjchem-193	192	17	(	(	PUNCT
eurjchem-193	192	18	12	12	NUM
eurjchem-193	192	19	)	)	PUNCT
eurjchem-193	192	20	.	.	PUNCT
eurjchem-193	193	1	acylation	acylation	NOUN
eurjchem-193	193	2	of	of	ADP
eurjchem-193	193	3	10	10	NUM
eurjchem-193	193	4	with	with	ADP
eurjchem-193	193	5	furoyl	furoyl	PROPN
eurjchem-193	193	6	chloride	chloride	NOUN
eurjchem-193	193	7	in	in	ADP
eurjchem-193	193	8	pyridine	pyridine	NOUN
eurjchem-193	193	9	gave	give	VERB
eurjchem-193	193	10	a	a	DET
eurjchem-193	193	11	yellow	yellow	ADJ
eurjchem-193	193	12	crystals	crystal	NOUN
eurjchem-193	193	13	product	product	NOUN
eurjchem-193	193	14	13	13	NUM
eurjchem-193	193	15	after	after	ADP
eurjchem-193	193	16	reflux	reflux	NOUN
eurjchem-193	193	17	for	for	ADP
eurjchem-193	193	18	four	four	NUM
eurjchem-193	193	19	hours	hour	NOUN
eurjchem-193	193	20	(	(	PUNCT
eurjchem-193	193	21	tlc	tlc	NOUN
eurjchem-193	193	22	)	)	PUNCT
eurjchem-193	193	23	.	.	PUNCT
eurjchem-193	194	1	full	full	ADJ
eurjchem-193	194	2	analysis	analysis	NOUN
eurjchem-193	194	3	for	for	ADP
eurjchem-193	194	4	13	13	NUM
eurjchem-193	194	5	using	use	VERB
eurjchem-193	194	6	spectroscopic	spectroscopic	ADJ
eurjchem-193	194	7	methods	method	NOUN
eurjchem-193	194	8	indicates	indicate	VERB
eurjchem-193	194	9	the	the	DET
eurjchem-193	194	10	incorporation	incorporation	NOUN
eurjchem-193	194	11	of	of	ADP
eurjchem-193	194	12	two	two	NUM
eurjchem-193	194	13	moles	mole	NOUN
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eurjchem-193	194	17	chloride	chloride	NOUN
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eurjchem-193	194	21	kcl	kcl	PROPN
eurjchem-193	194	22	.	.	PUNCT
eurjchem-193	195	1	references	reference	NOUN
eurjchem-193	195	2	[	[	X
eurjchem-193	195	3	1	1	NUM
eurjchem-193	195	4	]	]	PUNCT
eurjchem-193	195	5	.	.	PUNCT
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eurjchem-193	196	2	,	,	PUNCT
eurjchem-193	196	3	m.	m.	NOUN
eurjchem-193	196	4	a.	a.	PROPN
eurjchem-193	196	5	i.	i.	PROPN
eurjchem-193	196	6	;	;	PUNCT
eurjchem-193	196	7	soliman	soliman	PROPN
eurjchem-193	196	8	,	,	PUNCT
eurjchem-193	196	9	e.	e.	PROPN
eurjchem-193	196	10	a.	a.	PROPN
eurjchem-193	196	11	;	;	PUNCT
eurjchem-193	196	12	smith	smith	PROPN
eurjchem-193	196	13	,	,	PUNCT
eurjchem-193	196	14	m.	m.	PROPN
eurjchem-193	196	15	b.	b.	PROPN
eurjchem-193	196	16	;	;	PUNCT
eurjchem-193	196	17	mahmoud	mahmoud	PROPN
eurjchem-193	196	18	,	,	PUNCT
eurjchem-193	196	19	m.	m.	NOUN
eurjchem-193	196	20	r.	r.	PROPN
eurjchem-193	196	21	;	;	PUNCT
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eurjchem-193	196	23	,	,	PUNCT
eurjchem-193	196	24	m.	m.	PROPN
eurjchem-193	196	25	e.	e.	PROPN
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eurjchem-193	196	28	2004	2004	NUM
eurjchem-193	196	29	,	,	PUNCT
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eurjchem-193	196	33	.	.	PUNCT
eurjchem-193	197	1	[	[	X
eurjchem-193	197	2	2	2	NUM
eurjchem-193	197	3	]	]	PUNCT
eurjchem-193	197	4	.	.	PUNCT
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eurjchem-193	198	2	,	,	PUNCT
eurjchem-193	198	3	r.	r.	PROPN
eurjchem-193	198	4	p.	p.	PROPN
eurjchem-193	198	5	;	;	PUNCT
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eurjchem-193	198	7	,	,	PUNCT
eurjchem-193	198	8	b.	b.	PROPN
eurjchem-193	198	9	;	;	PUNCT
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eurjchem-193	198	11	,	,	PUNCT
eurjchem-193	198	12	g.	g.	PROPN
eurjchem-193	198	13	;	;	PUNCT
eurjchem-193	198	14	mahmoud	mahmoud	PROPN
eurjchem-193	198	15	,	,	PUNCT
eurjchem-193	198	16	m.	m.	NOUN
eurjchem-193	198	17	r.	r.	PROPN
eurjchem-193	198	18	;	;	PUNCT
eurjchem-193	198	19	mattoli	mattoli	PROPN
eurjchem-193	198	20	,	,	PUNCT
eurjchem-193	198	21	i.	i.	NOUN
eurjchem-193	198	22	;	;	PUNCT
eurjchem-193	198	23	sadeghpour	sadeghpour	ADJ
eurjchem-193	198	24	,	,	PUNCT
eurjchem-193	198	25	b.	b.	PROPN
eurjchem-193	198	26	m.	m.	PROPN
eurjchem-193	198	27	j.	j.	PROPN
eurjchem-193	198	28	med	med	PROPN
eurjchem-193	198	29	.	.	PROPN
eurjchem-193	198	30	chem	chem	PROPN
eurjchem-193	198	31	.	.	PUNCT
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eurjchem-193	199	2	,	,	PUNCT
eurjchem-193	199	3	37(5	37(5	NUM
eurjchem-193	199	4	)	)	PUNCT
eurjchem-193	199	5	,	,	PUNCT
eurjchem-193	199	6	647‐655	647‐655	NUM
eurjchem-193	199	7	.	.	PUNCT
eurjchem-193	200	1	[	[	X
eurjchem-193	200	2	3	3	NUM
eurjchem-193	200	3	]	]	PUNCT
eurjchem-193	200	4	.	.	PUNCT
eurjchem-193	201	1	mahmoud	mahmoud	PROPN
eurjchem-193	201	2	,	,	PUNCT
eurjchem-193	201	3	m.	m.	NOUN
eurjchem-193	201	4	r.	r.	PROPN
eurjchem-193	201	5	;	;	PUNCT
eurjchem-193	201	6	el‐bordany	el‐bordany	PROPN
eurjchem-193	201	7	e.	e.	PROPN
eurjchem-193	201	8	a.	a.	PROPN
eurjchem-193	201	9	a.	a.	PROPN
eurjchem-193	201	10	;	;	PUNCT
eurjchem-193	201	11	azab	azab	ADP
eurjchem-193	201	12	m.	m.	PROPN
eurjchem-193	201	13	e.	e.	PROPN
eurjchem-193	201	14	;	;	PUNCT
eurjchem-193	201	15	soliman	soliman	PROPN
eurjchem-193	201	16	e.	e.	PROPN
eurjchem-193	201	17	a.	a.	PROPN
eurjchem-193	201	18	phosphorus	phosphorus	PROPN
eurjchem-193	201	19	sulfur	sulfur	NOUN
eurjchem-193	201	20	2007	2007	NUM
eurjchem-193	201	21	,	,	PUNCT
eurjchem-193	201	22	181	181	NUM
eurjchem-193	201	23	,	,	PUNCT
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eurjchem-193	201	25	.	.	PUNCT
eurjchem-193	202	1	[	[	X
eurjchem-193	202	2	4	4	NUM
eurjchem-193	202	3	]	]	PUNCT
eurjchem-193	202	4	.	.	PUNCT
eurjchem-193	203	1	mahmoud	mahmoud	PROPN
eurjchem-193	203	2	,	,	PUNCT
eurjchem-193	203	3	m.	m.	NOUN
eurjchem-193	203	4	r.	r.	PROPN
eurjchem-193	203	5	;	;	PUNCT
eurjchem-193	203	6	el‐bordany	el‐bordany	PROPN
eurjchem-193	203	7	,	,	PUNCT
eurjchem-193	203	8	e.	e.	PROPN
eurjchem-193	203	9	a.	a.	PROPN
eurjchem-193	203	10	a.	a.	PROPN
eurjchem-193	203	11	;	;	PUNCT
eurjchem-193	203	12	hassan	hassan	PROPN
eurjchem-193	203	13	,	,	PUNCT
eurjchem-193	203	14	n.	n.	PROPN
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eurjchem-193	203	16	;	;	PUNCT
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eurjchem-193	203	18	el‐azm	el‐azm	PROPN
eurjchem-193	203	19	,	,	PUNCT
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eurjchem-193	203	21	s.	s.	PROPN
eurjchem-193	203	22	m.	m.	PROPN
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eurjchem-193	203	24	sulfur	sulfur	NOUN
eurjchem-193	203	25	2007	2007	NUM
eurjchem-193	203	26	,	,	PUNCT
eurjchem-193	203	27	182	182	NUM
eurjchem-193	203	28	,	,	PUNCT
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eurjchem-193	203	30	.	.	PUNCT
eurjchem-193	204	1	[	[	X
eurjchem-193	204	2	5	5	NUM
eurjchem-193	204	3	]	]	PUNCT
eurjchem-193	204	4	.	.	PUNCT
eurjchem-193	205	1	mahmoud	mahmoud	PROPN
eurjchem-193	205	2	,	,	PUNCT
eurjchem-193	205	3	m.	m.	NOUN
eurjchem-193	205	4	r.	r.	PROPN
eurjchem-193	205	5	;	;	PUNCT
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eurjchem-193	205	7	,	,	PUNCT
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eurjchem-193	205	9	m.	m.	PROPN
eurjchem-193	205	10	f.	f.	PROPN
eurjchem-193	205	11	;	;	PUNCT
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eurjchem-193	205	13	e.	e.	PROPN
eurjchem-193	205	14	a.	a.	PROPN
eurjchem-193	205	15	a.	a.	PROPN
eurjchem-193	205	16	;	;	PUNCT
eurjchem-193	205	17	soliman	soliman	PROPN
eurjchem-193	205	18	e.	e.	PROPN
eurjchem-193	205	19	a.	a.	PROPN
eurjchem-193	205	20	j.	j.	PROPN
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eurjchem-193	205	22	.	.	PUNCT
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eurjchem-193	206	2	.	.	PROPN
eurjchem-193	207	1	2007	2007	NUM
eurjchem-193	207	2	,	,	PUNCT
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eurjchem-193	207	4	,	,	PUNCT
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eurjchem-193	207	6	.	.	PUNCT
eurjchem-193	208	1	[	[	X
eurjchem-193	208	2	6	6	NUM
eurjchem-193	208	3	]	]	PUNCT
eurjchem-193	208	4	.	.	PUNCT
eurjchem-193	209	1	mahmoud	mahmoud	PROPN
eurjchem-193	209	2	,	,	PUNCT
eurjchem-193	209	3	m.	m.	NOUN
eurjchem-193	209	4	r.	r.	PROPN
eurjchem-193	209	5	;	;	PUNCT
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eurjchem-193	209	7	,	,	PUNCT
eurjchem-193	209	8	m.	m.	NOUN
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eurjchem-193	209	10	;	;	PUNCT
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eurjchem-193	209	12	,	,	PUNCT
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eurjchem-193	209	14	e.	e.	PROPN
eurjchem-193	209	15	j.	j.	PROPN
eurjchem-193	209	16	chem	chem	PROPN
eurjchem-193	209	17	.	.	PUNCT
eurjchem-193	210	1	res	re	NOUN
eurjchem-193	210	2	.	.	PROPN
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eurjchem-193	210	4	,	,	PUNCT
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eurjchem-193	210	8	.	.	PUNCT
eurjchem-193	211	1	[	[	X
eurjchem-193	211	2	7	7	NUM
eurjchem-193	211	3	]	]	PUNCT
eurjchem-193	211	4	.	.	PUNCT
eurjchem-193	212	1	mahmoud	mahmoud	PROPN
eurjchem-193	212	2	,	,	PUNCT
eurjchem-193	212	3	m.	m.	NOUN
eurjchem-193	212	4	r.	r.	PROPN
eurjchem-193	212	5	;	;	PUNCT
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eurjchem-193	212	7	,	,	PUNCT
eurjchem-193	212	8	m.	m.	NOUN
eurjchem-193	212	9	m.	m.	NOUN
eurjchem-193	212	10	;	;	PUNCT
eurjchem-193	212	11	farahat	farahat	PROPN
eurjchem-193	212	12	,	,	PUNCT
eurjchem-193	212	13	s.	s.	PROPN
eurjchem-193	212	14	e.	e.	PROPN
eurjchem-193	212	15	j.	j.	PROPN
eurjchem-193	212	16	chem	chem	PROPN
eurjchem-193	212	17	.	.	PUNCT
eurjchem-193	213	1	res	re	NOUN
eurjchem-193	213	2	.	.	PROPN
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eurjchem-193	213	4	,	,	PUNCT
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eurjchem-193	213	6	,	,	PUNCT
eurjchem-193	213	7	86‐88	86‐88	NUM
eurjchem-193	213	8	.	.	PUNCT
eurjchem-193	214	1	[	[	X
eurjchem-193	214	2	8	8	NUM
eurjchem-193	214	3	]	]	PUNCT
eurjchem-193	214	4	.	.	PUNCT
eurjchem-193	215	1	kambe	kambe	PROPN
eurjchem-193	215	2	,	,	PUNCT
eurjchem-193	215	3	s.	s.	PROPN
eurjchem-193	215	4	;	;	PUNCT
eurjchem-193	215	5	satio	satio	PROPN
eurjchem-193	215	6	,	,	PUNCT
eurjchem-193	215	7	k.	k.	PROPN
eurjchem-193	215	8	;	;	PUNCT
eurjchem-193	215	9	sakurai	sakurai	PROPN
eurjchem-193	215	10	,	,	PUNCT
eurjchem-193	215	11	a.	a.	NOUN
eurjchem-193	215	12	;	;	PUNCT
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eurjchem-193	215	14	,	,	PUNCT
eurjchem-193	215	15	h.	h.	NOUN
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eurjchem-193	215	18	,	,	PUNCT
eurjchem-193	215	19	7	7	NUM
eurjchem-193	215	20	,	,	PUNCT
eurjchem-193	215	21	531‐	531‐	NUM
eurjchem-193	215	22	532	532	NUM
eurjchem-193	215	23	.	.	PUNCT
eurjchem-193	216	1	[	[	X
eurjchem-193	216	2	9	9	NUM
eurjchem-193	216	3	]	]	PUNCT
eurjchem-193	216	4	.	.	PUNCT
eurjchem-193	217	1	madkour	madkour	PROPN
eurjchem-193	217	2	,	,	PUNCT
eurjchem-193	217	3	h.	h.	PROPN
eurjchem-193	217	4	m.	m.	PROPN
eurjchem-193	217	5	f.	f.	PROPN
eurjchem-193	217	6	;	;	PUNCT
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eurjchem-193	217	8	,	,	PUNCT
eurjchem-193	217	9	m.	m.	NOUN
eurjchem-193	217	10	r.	r.	PROPN
eurjchem-193	217	11	;	;	PUNCT
eurjchem-193	217	12	nassar	nassar	PROPN
eurjchem-193	217	13	,	,	PUNCT
eurjchem-193	217	14	m.	m.	PROPN
eurjchem-193	217	15	h.	h.	PROPN
eurjchem-193	217	16	;	;	PUNCT
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eurjchem-193	217	18	,	,	PUNCT
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eurjchem-193	217	20	m.	m.	NOUN
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eurjchem-193	217	24	,	,	PUNCT
eurjchem-193	217	25	21(6	21(6	NUM
eurjchem-193	217	26	)	)	PUNCT
eurjchem-193	217	27	,	,	PUNCT
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eurjchem-193	217	29	.	.	PUNCT
eurjchem-193	218	1	[	[	X
eurjchem-193	218	2	10	10	NUM
eurjchem-193	218	3	]	]	PUNCT
eurjchem-193	218	4	.	.	PUNCT
eurjchem-193	219	1	pretsh	pretsh	PROPN
eurjchem-193	219	2	,	,	PUNCT
eurjchem-193	219	3	e.	e.	PROPN
eurjchem-193	219	4	;	;	PUNCT
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eurjchem-193	219	6	,	,	PUNCT
eurjchem-193	219	7	t.	t.	PROPN
eurjchem-193	219	8	;	;	PUNCT
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eurjchem-193	219	10	,	,	PUNCT
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eurjchem-193	219	12	;	;	PUNCT
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eurjchem-193	219	14	,	,	PUNCT
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eurjchem-193	219	26	,	,	PUNCT
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eurjchem-193	219	28	,	,	PUNCT
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eurjchem-193	219	30	,	,	PUNCT
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eurjchem-193	219	33	.	.	PUNCT
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eurjchem-193	220	2	.	.	PUNCT
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eurjchem-193	221	2	and	and	CCONJ
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eurjchem-193	221	4	220	220	NUM
eurjchem-193	221	5	.	.	PUNCT
eurjchem-193	222	1	[	[	X
eurjchem-193	222	2	11	11	NUM
eurjchem-193	222	3	]	]	PUNCT
eurjchem-193	222	4	.	.	PUNCT
eurjchem-193	223	1	omar	omar	PROPN
eurjchem-193	223	2	,	,	PUNCT
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eurjchem-193	223	5	;	;	PUNCT
eurjchem-193	223	6	fouli	fouli	PROPN
eurjchem-193	223	7	,	,	PUNCT
eurjchem-193	223	8	f.	f.	PROPN
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eurjchem-193	223	10	;	;	PUNCT
eurjchem-193	223	11	elgarhi	elgarhi	PROPN
eurjchem-193	223	12	,	,	PUNCT
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eurjchem-193	223	14	z.	z.	PROPN
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eurjchem-193	223	16	.	.	PUNCT
eurjchem-193	224	1	chem	chem	PROPN
eurjchem-193	224	2	.	.	PUNCT
eurjchem-193	225	1	soc	soc	PROPN
eurjchem-193	225	2	.	.	PUNCT
eurjchem-193	226	1	jpn	jpn	PROPN
eurjchem-193	226	2	.	.	PROPN
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eurjchem-193	226	4	,	,	PUNCT
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eurjchem-193	226	6	,	,	PUNCT
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eurjchem-193	226	8	.	.	PUNCT
eurjchem-193	227	1	[	[	X
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eurjchem-193	227	3	]	]	PUNCT
eurjchem-193	227	4	.	.	PUNCT
eurjchem-193	228	1	raouf	raouf	PROPN
eurjchem-193	228	2	,	,	PUNCT
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eurjchem-193	228	5	a.	a.	PROPN
eurjchem-193	228	6	;	;	PUNCT
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eurjchem-193	228	8	,	,	PUNCT
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eurjchem-193	228	11	;	;	PUNCT
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eurjchem-193	228	13	,	,	PUNCT
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eurjchem-193	228	17	.	.	PUNCT
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eurjchem-193	229	2	.	.	PUNCT
eurjchem-193	230	1	acad	acad	PROPN
eurjchem-193	230	2	.	.	PUNCT
eurjchem-193	231	1	sci	sci	PROPN
eurjchem-193	231	2	.	.	PROPN
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eurjchem-193	231	4	,	,	PUNCT
eurjchem-193	231	5	87	87	NUM
eurjchem-193	231	6	,	,	PUNCT
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eurjchem-193	231	8	.	.	PUNCT
eurjchem-193	232	1	[	[	X
eurjchem-193	232	2	13	13	NUM
eurjchem-193	232	3	]	]	PUNCT
eurjchem-193	232	4	.	.	PUNCT
eurjchem-193	233	1	yiang	yiang	PROPN
eurjchem-193	233	2	,	,	PUNCT
eurjchem-193	233	3	y.	y.	PROPN
eurjchem-193	233	4	;	;	PUNCT
eurjchem-193	233	5	chem	chem	PROPN
eurjchem-193	233	6	,	,	PUNCT
eurjchem-193	233	7	j.	j.	PROPN
eurjchem-193	233	8	;	;	PUNCT
eurjchem-193	233	9	schinazi	schinazi	PROPN
eurjchem-193	233	10	,	,	PUNCT
eurjchem-193	233	11	r.	r.	PROPN
eurjchem-193	233	12	;	;	PUNCT
eurjchem-193	233	13	zhao	zhao	PROPN
eurjchem-193	233	14	,	,	PUNCT
eurjchem-193	233	15	k.	k.	PROPN
eurjchem-193	233	16	tetrahedron	tetrahedron	PROPN
eurjchem-193	233	17	lett	lett	PROPN
eurjchem-193	233	18	.	.	PUNCT
eurjchem-193	233	19	1995	1995	NUM
eurjchem-193	233	20	,	,	PUNCT
eurjchem-193	233	21	36(40	36(40	NUM
eurjchem-193	233	22	)	)	PUNCT
eurjchem-193	233	23	,	,	PUNCT
eurjchem-193	233	24	7193‐7196	7193‐7196	NUM
eurjchem-193	233	25	.	.	PUNCT
eurjchem-193	234	1	[	[	X
eurjchem-193	234	2	14	14	NUM
eurjchem-193	234	3	]	]	PUNCT
eurjchem-193	234	4	.	.	PUNCT
eurjchem-193	235	1	omar	omar	PROPN
eurjchem-193	235	2	,	,	PUNCT
eurjchem-193	235	3	m.	m.	NOUN
eurjchem-193	235	4	t.	t.	PROPN
eurjchem-193	235	5	;	;	PUNCT
eurjchem-193	235	6	habashy	habashy	ADJ
eurjchem-193	235	7	,	,	PUNCT
eurjchem-193	235	8	m.	m.	NOUN
eurjchem-193	235	9	m.	m.	NOUN
eurjchem-193	235	10	;	;	PUNCT
eurjchem-193	235	11	shaban	shaban	PROPN
eurjchem-193	235	12	,	,	PUNCT
eurjchem-193	235	13	m.	m.	PROPN
eurjchem-193	235	14	e.	e.	PROPN
eurjchem-193	235	15	;	;	PUNCT
eurjchem-193	235	16	kasem	kasem	PROPN
eurjchem-193	235	17	,	,	PUNCT
eurjchem-193	235	18	m.	m.	NOUN
eurjchem-193	235	19	a.	a.	NOUN
eurjchem-193	235	20	synthesis	synthesis	NOUN
eurjchem-193	235	21	1981	1981	NUM
eurjchem-193	235	22	,	,	PUNCT
eurjchem-193	235	23	4	4	NUM
eurjchem-193	235	24	,	,	PUNCT
eurjchem-193	235	25	318‐318	318‐318	NUM
eurjchem-193	235	26	.	.	PUNCT