id sid tid token lemma pos eurjchem-20 1 1 microsoft microsoft PROPN eurjchem-20 1 2 word word PROPN eurjchem-20 1 3 european_journal_of_chemistry_1_4_2010_297_301_20 european_journal_of_chemistry_1_4_2010_297_301_20 PROPN eurjchem-20 1 4 european european ADJ eurjchem-20 1 5     SPACE eurjchem-20 1 6 journal journal NOUN eurjchem-20 1 7     SPACE eurjchem-20 1 8 of of ADP eurjchem-20 1 9     SPACE eurjchem-20 1 10 chemistry chemistry NOUN eurjchem-20 1 11     SPACE eurjchem-20 1 12 1 1 NUM eurjchem-20 1 13     SPACE eurjchem-20 1 14 ( ( PUNCT eurjchem-20 1 15 4 4 NUM eurjchem-20 1 16 ) ) PUNCT eurjchem-20 1 17     SPACE eurjchem-20 1 18 ( ( PUNCT eurjchem-20 1 19 2010 2010 NUM eurjchem-20 1 20 ) ) PUNCT eurjchem-20 1 21     SPACE eurjchem-20 1 22 297‐301 297‐301 NUM eurjchem-20 1 23         SPACE eurjchem-20 1 24 european european ADJ eurjchem-20 1 25     SPACE eurjchem-20 1 26 journal journal NOUN eurjchem-20 1 27     SPACE eurjchem-20 1 28 of of ADP eurjchem-20 1 29     SPACE eurjchem-20 1 30 chemistry chemistry NOUN eurjchem-20 1 31     SPACE eurjchem-20 1 32 issn issn VERB eurjchem-20 1 33     SPACE eurjchem-20 1 34 2153‐2249 2153‐2249 NUM eurjchem-20 1 35     SPACE eurjchem-20 1 36 ( ( PUNCT eurjchem-20 1 37 print print NOUN eurjchem-20 1 38 ) ) PUNCT eurjchem-20 1 39     SPACE eurjchem-20 1 40 / / SYM eurjchem-20 1 41     SPACE eurjchem-20 1 42 issn issn VERB eurjchem-20 1 43     SPACE eurjchem-20 1 44 2153‐2257 2153‐2257 NUM eurjchem-20 1 45     SPACE eurjchem-20 1 46 ( ( PUNCT eurjchem-20 1 47 online online ADJ eurjchem-20 1 48 ) ) PUNCT eurjchem-20 1 49     SPACE eurjchem-20 1 50   NOUN eurjchem-20 1 51     SPACE eurjchem-20 1 52 2010 2010 NUM eurjchem-20 1 53     SPACE eurjchem-20 1 54 eurjchem eurjchem NOUN eurjchem-20 1 55     SPACE eurjchem-20 1 56 doi:10.5155 doi:10.5155 PROPN eurjchem-20 1 57 / / SYM eurjchem-20 1 58 eurjchem.1.4.297‐301.20 eurjchem.1.4.297‐301.20 NUM eurjchem-20 1 59                 SPACE eurjchem-20 1 60 european european ADJ eurjchem-20 1 61     SPACE eurjchem-20 1 62 journal journal NOUN eurjchem-20 1 63     SPACE eurjchem-20 1 64 of of ADP eurjchem-20 1 65     SPACE eurjchem-20 1 66 chemistry chemistry NOUN eurjchem-20 1 67     SPACE eurjchem-20 1 68 journal journal NOUN eurjchem-20 1 69     SPACE eurjchem-20 1 70 homepage homepage NOUN eurjchem-20 1 71 : : PUNCT eurjchem-20 1 72     SPACE eurjchem-20 1 73 www.eurjchem.com www.eurjchem.com NOUN eurjchem-20 1 74                     SPACE eurjchem-20 1 75 synthesis synthesis NOUN eurjchem-20 1 76     SPACE eurjchem-20 1 77 and and CCONJ eurjchem-20 1 78     SPACE eurjchem-20 1 79 bioactivity bioactivity NOUN eurjchem-20 1 80     SPACE eurjchem-20 1 81 of of ADP eurjchem-20 1 82     SPACE eurjchem-20 1 83 phosphorylated phosphorylate VERB eurjchem-20 1 84     SPACE eurjchem-20 1 85 derivatives derivative NOUN eurjchem-20 1 86     SPACE eurjchem-20 1 87 of of ADP eurjchem-20 1 88     SPACE eurjchem-20 1 89 stavudine stavudine ADJ eurjchem-20 1 90     SPACE eurjchem-20 1 91 alahari alahari PROPN eurjchem-20 1 92     SPACE eurjchem-20 1 93 janardhan janardhan PROPN eurjchem-20 1 94     SPACE eurjchem-20 1 95 raoa raoa PROPN eurjchem-20 1 96 , , PUNCT eurjchem-20 1 97     SPACE eurjchem-20 1 98 valasani valasani NOUN eurjchem-20 1 99     SPACE eurjchem-20 1 100 koteswara koteswara PROPN eurjchem-20 1 101     SPACE eurjchem-20 1 102 raoa raoa PROPN eurjchem-20 1 103 , , PUNCT eurjchem-20 1 104     SPACE eurjchem-20 1 105 pasupuleti pasupuleti ADJ eurjchem-20 1 106     SPACE eurjchem-20 1 107 visweswara visweswara PROPN eurjchem-20 1 108     SPACE eurjchem-20 1 109 raob raob NOUN eurjchem-20 1 110 , , PUNCT eurjchem-20 1 111       SPACE eurjchem-20 1 112 chamarthi chamarthi NOUN eurjchem-20 1 113     SPACE eurjchem-20 1 114 naga naga NOUN eurjchem-20 1 115     SPACE eurjchem-20 1 116 rajua rajua NOUN eurjchem-20 1 117 , , PUNCT eurjchem-20 1 118 * * PUNCT eurjchem-20 1 119     SPACE eurjchem-20 1 120 and and CCONJ eurjchem-20 1 121     SPACE eurjchem-20 1 122 sunil sunil PROPN eurjchem-20 1 123     SPACE eurjchem-20 1 124 kumar kumar PROPN eurjchem-20 1 125     SPACE eurjchem-20 1 126 ghoshc ghoshc PROPN eurjchem-20 1 127     SPACE eurjchem-20 1 128 a a DET eurjchem-20 1 129     SPACE eurjchem-20 1 130 department department NOUN eurjchem-20 1 131     SPACE eurjchem-20 1 132 of of ADP eurjchem-20 1 133     SPACE eurjchem-20 1 134 chemistry chemistry NOUN eurjchem-20 1 135 , , PUNCT eurjchem-20 1 136     SPACE eurjchem-20 1 137 sri sri NOUN eurjchem-20 1 138     SPACE eurjchem-20 1 139 venkateswara venkateswara PROPN eurjchem-20 1 140     SPACE eurjchem-20 1 141 university university NOUN eurjchem-20 1 142 , , PUNCT eurjchem-20 1 143     SPACE eurjchem-20 1 144 tirupati tirupati NOUN eurjchem-20 1 145 , , PUNCT eurjchem-20 1 146     SPACE eurjchem-20 1 147 in­517502 in­517502 PROPN eurjchem-20 1 148 , , PUNCT eurjchem-20 1 149     SPACE eurjchem-20 1 150 india india PROPN eurjchem-20 1 151       SPACE eurjchem-20 1 152 b b PROPN eurjchem-20 1 153     SPACE eurjchem-20 1 154 department department NOUN eurjchem-20 1 155     SPACE eurjchem-20 1 156 of of ADP eurjchem-20 1 157     SPACE eurjchem-20 1 158 biotechnology biotechnology NOUN eurjchem-20 1 159 , , PUNCT eurjchem-20 1 160     SPACE eurjchem-20 1 161 sri sri NOUN eurjchem-20 1 162     SPACE eurjchem-20 1 163 venkateswara venkateswara PROPN eurjchem-20 1 164     SPACE eurjchem-20 1 165 university university NOUN eurjchem-20 1 166 , , PUNCT eurjchem-20 1 167     SPACE eurjchem-20 1 168 tirupati tirupati NOUN eurjchem-20 1 169 , , PUNCT eurjchem-20 1 170     SPACE eurjchem-20 1 171 in­517502 in­517502 PROPN eurjchem-20 1 172 , , PUNCT eurjchem-20 1 173     SPACE eurjchem-20 1 174 india india PROPN eurjchem-20 1 175     SPACE eurjchem-20 1 176 c c PROPN eurjchem-20 1 177     SPACE eurjchem-20 1 178 bio­organic bio­organic ADJ eurjchem-20 1 179     SPACE eurjchem-20 1 180 division division NOUN eurjchem-20 1 181 , , PUNCT eurjchem-20 1 182     SPACE eurjchem-20 1 183 bhabha bhabha NOUN eurjchem-20 1 184     SPACE eurjchem-20 1 185 atomic atomic ADJ eurjchem-20 1 186     SPACE eurjchem-20 1 187 research research NOUN eurjchem-20 1 188     SPACE eurjchem-20 1 189 centre centre NOUN eurjchem-20 1 190 , , PUNCT eurjchem-20 1 191     SPACE eurjchem-20 1 192 mumbai mumbai PROPN eurjchem-20 1 193 , , PUNCT eurjchem-20 1 194     SPACE eurjchem-20 1 195 in­400085 in­400085 PROPN eurjchem-20 1 196 , , PUNCT eurjchem-20 1 197     SPACE eurjchem-20 1 198 india india PROPN eurjchem-20 1 199     SPACE eurjchem-20 1 200 * * PROPN eurjchem-20 1 201 corresponding correspond VERB eurjchem-20 1 202     SPACE eurjchem-20 1 203 author author NOUN eurjchem-20 1 204     SPACE eurjchem-20 1 205 at at ADP eurjchem-20 1 206 : : PUNCT eurjchem-20 1 207     SPACE eurjchem-20 1 208 department department NOUN eurjchem-20 1 209     SPACE eurjchem-20 1 210 of of ADP eurjchem-20 1 211     SPACE eurjchem-20 1 212 chemistry chemistry NOUN eurjchem-20 1 213 , , PUNCT eurjchem-20 1 214     SPACE eurjchem-20 1 215 sri sri NOUN eurjchem-20 1 216     SPACE eurjchem-20 1 217 venkateswara venkateswara PROPN eurjchem-20 1 218     SPACE eurjchem-20 1 219 university university NOUN eurjchem-20 1 220 , , PUNCT eurjchem-20 1 221     SPACE eurjchem-20 1 222 tirupati tirupati NOUN eurjchem-20 1 223 , , PUNCT eurjchem-20 1 224     SPACE eurjchem-20 1 225 in­517502 in­517502 PROPN eurjchem-20 1 226 , , PUNCT eurjchem-20 1 227     SPACE eurjchem-20 1 228 india india PROPN eurjchem-20 1 229 . . PUNCT eurjchem-20 1 230     SPACE eurjchem-20 2 1 tel tel PROPN eurjchem-20 2 2 . . PUNCT eurjchem-20 2 3 : : PUNCT eurjchem-20 2 4     SPACE eurjchem-20 3 1 +91.877.2249666 +91.877.2249666 NUM eurjchem-20 3 2 ; ; PUNCT eurjchem-20 3 3     SPACE eurjchem-20 3 4 fax fax NOUN eurjchem-20 3 5 : : PUNCT eurjchem-20 3 6     SPACE eurjchem-20 3 7 +91.877.2225211 +91.877.2225211 PROPN eurjchem-20 3 8 . . PUNCT eurjchem-20 3 9     SPACE eurjchem-20 3 10 e­mail e­mail NOUN eurjchem-20 3 11     SPACE eurjchem-20 3 12 address address NOUN eurjchem-20 3 13 : : PUNCT eurjchem-20 3 14     SPACE eurjchem-20 3 15 rajuchamarthi10@gmail.com rajuchamarthi10@gmail.com X eurjchem-20 3 16       SPACE eurjchem-20 3 17 ( ( PUNCT eurjchem-20 3 18 c. c. PROPN eurjchem-20 3 19     SPACE eurjchem-20 3 20 n. n. PROPN eurjchem-20 3 21     SPACE eurjchem-20 3 22 raju raju PROPN eurjchem-20 3 23 ) ) PUNCT eurjchem-20 3 24 . . PUNCT eurjchem-20 3 25                                 SPACE eurjchem-20 4 1 article article NOUN eurjchem-20 4 2     SPACE eurjchem-20 4 3 information information NOUN eurjchem-20 4 4         SPACE eurjchem-20 4 5 abstract abstract ADJ eurjchem-20 4 6 received receive VERB eurjchem-20 4 7 : : PUNCT eurjchem-20 4 8     SPACE eurjchem-20 4 9 28 28 NUM eurjchem-20 4 10     SPACE eurjchem-20 4 11 march march PROPN eurjchem-20 4 12     SPACE eurjchem-20 4 13 2010 2010 NUM eurjchem-20 4 14     SPACE eurjchem-20 4 15 received receive VERB eurjchem-20 4 16     SPACE eurjchem-20 4 17 in in ADP eurjchem-20 4 18     SPACE eurjchem-20 4 19 revised revise VERB eurjchem-20 4 20     SPACE eurjchem-20 4 21 form form NOUN eurjchem-20 4 22 : : PUNCT eurjchem-20 4 23     SPACE eurjchem-20 4 24 13 13 NUM eurjchem-20 4 25     SPACE eurjchem-20 4 26 august august PROPN eurjchem-20 4 27     SPACE eurjchem-20 4 28 2010 2010 NUM eurjchem-20 4 29     SPACE eurjchem-20 4 30 accepted accept VERB eurjchem-20 4 31 : : PUNCT eurjchem-20 4 32     SPACE eurjchem-20 4 33 20 20 NUM eurjchem-20 4 34     SPACE eurjchem-20 4 35 september september PROPN eurjchem-20 4 36     SPACE eurjchem-20 4 37 2010 2010 NUM eurjchem-20 4 38     SPACE eurjchem-20 4 39 online online NOUN eurjchem-20 4 40 : : PUNCT eurjchem-20 4 41     SPACE eurjchem-20 4 42 31 31 NUM eurjchem-20 4 43     SPACE eurjchem-20 4 44 december december PROPN eurjchem-20 4 45     SPACE eurjchem-20 4 46 2010 2010 NUM eurjchem-20 4 47     SPACE eurjchem-20 4 48 keywords keyword VERB eurjchem-20 4 49         SPACE eurjchem-20 4 50 novel novel NOUN eurjchem-20 4 51     SPACE eurjchem-20 4 52 phosphorylated phosphorylate VERB eurjchem-20 4 53     SPACE eurjchem-20 4 54 derivatives derivative NOUN eurjchem-20 4 55     SPACE eurjchem-20 4 56 of of ADP eurjchem-20 4 57     SPACE eurjchem-20 4 58 stavudine stavudine NOUN eurjchem-20 4 59     SPACE eurjchem-20 4 60 were be AUX eurjchem-20 4 61     SPACE eurjchem-20 4 62 synthesized synthesize VERB eurjchem-20 4 63     SPACE eurjchem-20 4 64 by by ADP eurjchem-20 4 65     SPACE eurjchem-20 4 66 the the DET eurjchem-20 4 67     SPACE eurjchem-20 4 68 reaction reaction NOUN eurjchem-20 4 69     SPACE eurjchem-20 4 70 of of ADP eurjchem-20 4 71     SPACE eurjchem-20 4 72 bis(2‐ bis(2‐ PROPN eurjchem-20 4 73 chloroethyl)phosphoramidic chloroethyl)phosphoramidic ADJ eurjchem-20 4 74     SPACE eurjchem-20 4 75 dichloride/4‐nitrophenyl dichloride/4‐nitrophenyl NOUN eurjchem-20 4 76     SPACE eurjchem-20 4 77 phosphorodichloridate phosphorodichloridate NOUN eurjchem-20 4 78     SPACE eurjchem-20 4 79 with with ADP eurjchem-20 4 80     SPACE eurjchem-20 4 81 various various ADJ eurjchem-20 4 82     SPACE eurjchem-20 4 83 cyclic cyclic ADJ eurjchem-20 4 84     SPACE eurjchem-20 4 85 amines amine NOUN eurjchem-20 4 86     SPACE eurjchem-20 4 87 and and CCONJ eurjchem-20 4 88     SPACE eurjchem-20 4 89 amino amino NOUN eurjchem-20 4 90     SPACE eurjchem-20 4 91 acid acid NOUN eurjchem-20 4 92     SPACE eurjchem-20 4 93 esters ester NOUN eurjchem-20 4 94     SPACE eurjchem-20 4 95 in in ADP eurjchem-20 4 96     SPACE eurjchem-20 4 97 the the DET eurjchem-20 4 98     SPACE eurjchem-20 4 99 presence presence NOUN eurjchem-20 4 100     SPACE eurjchem-20 4 101 of of ADP eurjchem-20 4 102     SPACE eurjchem-20 4 103 triethylamine triethylamine NOUN eurjchem-20 4 104     SPACE eurjchem-20 4 105 in in ADP eurjchem-20 4 106     SPACE eurjchem-20 4 107 dry dry ADJ eurjchem-20 4 108     SPACE eurjchem-20 4 109 tetrahydrofuran tetrahydrofuran NOUN eurjchem-20 4 110     SPACE eurjchem-20 4 111 through through ADP eurjchem-20 4 112     SPACE eurjchem-20 4 113 the the DET eurjchem-20 4 114     SPACE eurjchem-20 4 115 corresponding corresponding ADJ eurjchem-20 4 116     SPACE eurjchem-20 4 117 monochloride monochloride NOUN eurjchem-20 4 118     SPACE eurjchem-20 4 119 intermediates intermediate NOUN eurjchem-20 4 120     SPACE eurjchem-20 4 121 2a‐l 2a‐l NOUN eurjchem-20 4 122 . . PUNCT eurjchem-20 4 123     SPACE eurjchem-20 4 124 further further ADJ eurjchem-20 4 125     SPACE eurjchem-20 4 126 reaction reaction NOUN eurjchem-20 4 127     SPACE eurjchem-20 4 128 of of ADP eurjchem-20 4 129     SPACE eurjchem-20 4 130 the the DET eurjchem-20 4 131     SPACE eurjchem-20 4 132 intermediates intermediate NOUN eurjchem-20 4 133     SPACE eurjchem-20 4 134 2a‐l 2a‐l NOUN eurjchem-20 4 135     SPACE eurjchem-20 4 136 with with ADP eurjchem-20 4 137     SPACE eurjchem-20 4 138 stavudine stavudine NOUN eurjchem-20 4 139     SPACE eurjchem-20 4 140 in in ADP eurjchem-20 4 141     SPACE eurjchem-20 4 142 tetrahydrofuran tetrahydrofuran NOUN eurjchem-20 4 143     SPACE eurjchem-20 4 144 and and CCONJ eurjchem-20 4 145     SPACE eurjchem-20 4 146 pyridine pyridine NOUN eurjchem-20 4 147     SPACE eurjchem-20 4 148 in in ADP eurjchem-20 4 149     SPACE eurjchem-20 4 150 the the DET eurjchem-20 4 151     SPACE eurjchem-20 4 152 presence presence NOUN eurjchem-20 4 153     SPACE eurjchem-20 4 154 of of ADP eurjchem-20 4 155     SPACE eurjchem-20 4 156 triethylamine triethylamine NOUN eurjchem-20 4 157     SPACE eurjchem-20 4 158 formed form VERB eurjchem-20 4 159     SPACE eurjchem-20 4 160 the the DET eurjchem-20 4 161     SPACE eurjchem-20 4 162 title title NOUN eurjchem-20 4 163     SPACE eurjchem-20 4 164 compounds compound VERB eurjchem-20 4 165     SPACE eurjchem-20 4 166 4a‐l 4a‐l NOUN eurjchem-20 4 167 . . PUNCT eurjchem-20 4 168     SPACE eurjchem-20 5 1 their their PRON eurjchem-20 5 2     SPACE eurjchem-20 5 3 structures structure NOUN eurjchem-20 5 4     SPACE eurjchem-20 5 5 were be AUX eurjchem-20 5 6     SPACE eurjchem-20 5 7 characterized characterize VERB eurjchem-20 5 8     SPACE eurjchem-20 5 9 by by ADP eurjchem-20 5 10     SPACE eurjchem-20 5 11 ir ir PROPN eurjchem-20 5 12 , , PUNCT eurjchem-20 5 13     SPACE eurjchem-20 5 14 1h‐ 1h‐ NUM eurjchem-20 5 15 , , PUNCT eurjchem-20 5 16     SPACE eurjchem-20 5 17 13c‐ 13c‐ NOUN eurjchem-20 5 18 , , PUNCT eurjchem-20 5 19     SPACE eurjchem-20 5 20 31p‐nmr 31p‐nmr NOUN eurjchem-20 5 21     SPACE eurjchem-20 5 22 and and CCONJ eurjchem-20 5 23     SPACE eurjchem-20 5 24 mass mass PROPN eurjchem-20 5 25     SPACE eurjchem-20 5 26 spectral spectral ADJ eurjchem-20 5 27     SPACE eurjchem-20 5 28 data datum NOUN eurjchem-20 5 29     SPACE eurjchem-20 5 30 analyses analysis NOUN eurjchem-20 5 31 . . PUNCT eurjchem-20 5 32     SPACE eurjchem-20 6 1 they they PRON eurjchem-20 6 2     SPACE eurjchem-20 6 3 exhibited exhibit VERB eurjchem-20 6 4     SPACE eurjchem-20 6 5 good good ADJ eurjchem-20 6 6     SPACE eurjchem-20 6 7 antibacterial antibacterial NOUN eurjchem-20 6 8     SPACE eurjchem-20 6 9 and and CCONJ eurjchem-20 6 10     SPACE eurjchem-20 6 11 antioxidant antioxidant ADJ eurjchem-20 6 12     SPACE eurjchem-20 6 13 activities activity NOUN eurjchem-20 6 14 . . PUNCT eurjchem-20 6 15     SPACE eurjchem-20 7 1 their their PRON eurjchem-20 7 2     SPACE eurjchem-20 7 3 bioactivity bioactivity NOUN eurjchem-20 7 4     SPACE eurjchem-20 7 5 was be AUX eurjchem-20 7 6     SPACE eurjchem-20 7 7 greatly greatly ADV eurjchem-20 7 8     SPACE eurjchem-20 7 9 influenced influence VERB eurjchem-20 7 10     SPACE eurjchem-20 7 11 by by ADP eurjchem-20 7 12     SPACE eurjchem-20 7 13 the the DET eurjchem-20 7 14     SPACE eurjchem-20 7 15 different different ADJ eurjchem-20 7 16     SPACE eurjchem-20 7 17 groups group NOUN eurjchem-20 7 18     SPACE eurjchem-20 7 19 present present ADJ eurjchem-20 7 20     SPACE eurjchem-20 7 21 at at ADP eurjchem-20 7 22     SPACE eurjchem-20 7 23 the the DET eurjchem-20 7 24     SPACE eurjchem-20 7 25 phosphorus phosphorus NOUN eurjchem-20 7 26 . . PUNCT eurjchem-20 7 27     SPACE eurjchem-20 8 1 phosphorylated phosphorylate VERB eurjchem-20 8 2     SPACE eurjchem-20 8 3 derivatives derivative NOUN eurjchem-20 8 4     SPACE eurjchem-20 8 5 of of ADP eurjchem-20 8 6     SPACE eurjchem-20 8 7 stavudine stavudine ADJ eurjchem-20 8 8     SPACE eurjchem-20 8 9 gram‐positive gram‐positive ADJ eurjchem-20 8 10     SPACE eurjchem-20 8 11 bacteria bacteria NOUN eurjchem-20 8 12     SPACE eurjchem-20 8 13 gram‐negative gram‐negative PROPN eurjchem-20 8 14     SPACE eurjchem-20 8 15 bacteria bacteria NOUN eurjchem-20 8 16     SPACE eurjchem-20 8 17 antibacterial antibacterial ADJ eurjchem-20 8 18     SPACE eurjchem-20 8 19 activity activity NOUN eurjchem-20 8 20     SPACE eurjchem-20 8 21 antioxidant antioxidant NOUN eurjchem-20 8 22     SPACE eurjchem-20 8 23 activity activity NOUN eurjchem-20 8 24         SPACE eurjchem-20 8 25 1 1 NUM eurjchem-20 8 26 . . PUNCT eurjchem-20 8 27     SPACE eurjchem-20 8 28 introduction introduction NOUN eurjchem-20 8 29         SPACE eurjchem-20 8 30 nucleoside nucleoside NOUN eurjchem-20 8 31     SPACE eurjchem-20 8 32 analogues analogue NOUN eurjchem-20 8 33     SPACE eurjchem-20 8 34 continue continue VERB eurjchem-20 8 35     SPACE eurjchem-20 8 36 to to PART eurjchem-20 8 37     SPACE eurjchem-20 8 38 dominate dominate VERB eurjchem-20 8 39     SPACE eurjchem-20 8 40 over over ADP eurjchem-20 8 41     SPACE eurjchem-20 8 42 other other ADJ eurjchem-20 8 43     SPACE eurjchem-20 8 44 drugs drug NOUN eurjchem-20 8 45     SPACE eurjchem-20 8 46 in in ADP eurjchem-20 8 47     SPACE eurjchem-20 8 48 chemotherapy chemotherapy NOUN eurjchem-20 8 49     SPACE eurjchem-20 8 50 of of ADP eurjchem-20 8 51     SPACE eurjchem-20 8 52 cancer cancer NOUN eurjchem-20 8 53     SPACE eurjchem-20 8 54 and and CCONJ eurjchem-20 8 55     SPACE eurjchem-20 8 56 antiviral antiviral ADJ eurjchem-20 8 57     SPACE eurjchem-20 8 58 diseases disease NOUN eurjchem-20 8 59 . . PUNCT eurjchem-20 8 60     SPACE eurjchem-20 9 1 some some PRON eurjchem-20 9 2     SPACE eurjchem-20 9 3 of of ADP eurjchem-20 9 4     SPACE eurjchem-20 9 5 the the DET eurjchem-20 9 6     SPACE eurjchem-20 9 7 nucleoside nucleoside NOUN eurjchem-20 9 8     SPACE eurjchem-20 9 9 analogues analogue NOUN eurjchem-20 9 10     SPACE eurjchem-20 9 11 with with ADP eurjchem-20 9 12     SPACE eurjchem-20 9 13 such such ADJ eurjchem-20 9 14     SPACE eurjchem-20 9 15 an an DET eurjchem-20 9 16     SPACE eurjchem-20 9 17 activity activity NOUN eurjchem-20 9 18     SPACE eurjchem-20 9 19 are be AUX eurjchem-20 9 20     SPACE eurjchem-20 9 21 ddc ddc NOUN eurjchem-20 9 22 , , PUNCT eurjchem-20 9 23     SPACE eurjchem-20 9 24 fmau fmau NOUN eurjchem-20 9 25 , , PUNCT eurjchem-20 9 26     SPACE eurjchem-20 9 27 oddc oddc NOUN eurjchem-20 9 28 , , PUNCT eurjchem-20 9 29     SPACE eurjchem-20 9 30 bch‐189 bch‐189 PROPN eurjchem-20 9 31 , , PUNCT eurjchem-20 9 32     SPACE eurjchem-20 9 33 azt azt PROPN eurjchem-20 9 34 . . PUNCT eurjchem-20 9 35     SPACE eurjchem-20 9 36 stavudine stavudine NOUN eurjchem-20 9 37     SPACE eurjchem-20 9 38 ( ( PUNCT eurjchem-20 9 39 2',3'‐dideoxy‐2',3'‐ 2',3'‐dideoxy‐2',3'‐ ADJ eurjchem-20 9 40 didehydrothymidine didehydrothymidine NOUN eurjchem-20 9 41 ; ; PUNCT eurjchem-20 9 42     SPACE eurjchem-20 9 43 d4 d4 PROPN eurjchem-20 9 44 t t PROPN eurjchem-20 9 45 ) ) PUNCT eurjchem-20 9 46     SPACE eurjchem-20 9 47 is be AUX eurjchem-20 9 48     SPACE eurjchem-20 9 49 licensed licensed ADJ eurjchem-20 9 50     SPACE eurjchem-20 9 51 for for ADP eurjchem-20 9 52     SPACE eurjchem-20 9 53 use use NOUN eurjchem-20 9 54     SPACE eurjchem-20 9 55 in in ADP eurjchem-20 9 56     SPACE eurjchem-20 9 57 the the DET eurjchem-20 9 58     SPACE eurjchem-20 9 59 human human ADJ eurjchem-20 9 60     SPACE eurjchem-20 9 61 immunodeficiency immunodeficiency NOUN eurjchem-20 9 62     SPACE eurjchem-20 9 63 virus virus NOUN eurjchem-20 9 64     SPACE eurjchem-20 9 65 ( ( PUNCT eurjchem-20 9 66 hiv hiv PROPN eurjchem-20 9 67 ) ) PUNCT eurjchem-20 9 68     SPACE eurjchem-20 9 69 infection infection NOUN eurjchem-20 9 70     SPACE eurjchem-20 10 1 [ [ X eurjchem-20 10 2 1,2 1,2 NUM eurjchem-20 10 3 ] ] PUNCT eurjchem-20 10 4 . . PUNCT eurjchem-20 10 5     SPACE eurjchem-20 10 6 nucleosides nucleoside VERB eurjchem-20 10 7     SPACE eurjchem-20 10 8 to to PART eurjchem-20 10 9     SPACE eurjchem-20 10 10 become become VERB eurjchem-20 10 11     SPACE eurjchem-20 10 12 bioactive bioactive NOUN eurjchem-20 10 13     SPACE eurjchem-20 10 14 are be AUX eurjchem-20 10 15     SPACE eurjchem-20 10 16 to to PART eurjchem-20 10 17     SPACE eurjchem-20 10 18 be be AUX eurjchem-20 10 19     SPACE eurjchem-20 10 20 phosphorylated phosphorylate VERB eurjchem-20 10 21     SPACE eurjchem-20 10 22 by by ADP eurjchem-20 10 23     SPACE eurjchem-20 10 24 cellular cellular ADJ eurjchem-20 10 25     SPACE eurjchem-20 10 26 kinases kinase NOUN eurjchem-20 10 27     SPACE eurjchem-20 10 28 to to PART eurjchem-20 10 29     SPACE eurjchem-20 10 30 give give VERB eurjchem-20 10 31     SPACE eurjchem-20 10 32 successively successively ADV eurjchem-20 10 33     SPACE eurjchem-20 10 34 corresponding corresponding ADJ eurjchem-20 10 35     SPACE eurjchem-20 10 36 5'‐mono‐ 5'‐mono‐ NOUN eurjchem-20 10 37 , , PUNCT eurjchem-20 10 38     SPACE eurjchem-20 10 39 ‐di ‐di NOUN eurjchem-20 10 40 , , PUNCT eurjchem-20 10 41     SPACE eurjchem-20 10 42 and and CCONJ eurjchem-20 10 43     SPACE eurjchem-20 10 44 – – PUNCT eurjchem-20 10 45 triphos‐ triphos‐ NOUN eurjchem-20 10 46 phates phate NOUN eurjchem-20 10 47 . . PUNCT eurjchem-20 10 48     SPACE eurjchem-20 11 1 it it PRON eurjchem-20 11 2     SPACE eurjchem-20 11 3 is be AUX eurjchem-20 11 4     SPACE eurjchem-20 11 5 reported report VERB eurjchem-20 11 6     SPACE eurjchem-20 11 7 that that SCONJ eurjchem-20 11 8     SPACE eurjchem-20 11 9 intracellular intracellular ADJ eurjchem-20 11 10     SPACE eurjchem-20 11 11 phosphorylation phosphorylation NOUN eurjchem-20 11 12     SPACE eurjchem-20 11 13 of of ADP eurjchem-20 11 14     SPACE eurjchem-20 11 15 stavudine stavudine NOUN eurjchem-20 11 16     SPACE eurjchem-20 11 17 via via ADP eurjchem-20 11 18     SPACE eurjchem-20 11 19 monophosphate monophosphate NOUN eurjchem-20 11 20     SPACE eurjchem-20 11 21 and and CCONJ eurjchem-20 11 22     SPACE eurjchem-20 11 23 diphosphate diphosphate NOUN eurjchem-20 11 24 , , PUNCT eurjchem-20 11 25     SPACE eurjchem-20 11 26 to to ADP eurjchem-20 11 27     SPACE eurjchem-20 11 28 the the DET eurjchem-20 11 29     SPACE eurjchem-20 11 30 active active ADJ eurjchem-20 11 31     SPACE eurjchem-20 11 32 triphosphate triphosphate NOUN eurjchem-20 11 33     SPACE eurjchem-20 11 34 anabolite anabolite NOUN eurjchem-20 11 35     SPACE eurjchem-20 11 36 which which PRON eurjchem-20 11 37     SPACE eurjchem-20 11 38 inhibits inhibit VERB eurjchem-20 11 39     SPACE eurjchem-20 11 40 hiv hiv PROPN eurjchem-20 11 41     SPACE eurjchem-20 11 42 reverse reverse NOUN eurjchem-20 11 43     SPACE eurjchem-20 11 44 transcriptase transcriptase NOUN eurjchem-20 11 45     SPACE eurjchem-20 11 46 and and CCONJ eurjchem-20 11 47     SPACE eurjchem-20 11 48 terminates terminate VERB eurjchem-20 11 49     SPACE eurjchem-20 11 50 the the DET eurjchem-20 11 51     SPACE eurjchem-20 11 52 elongating elongate VERB eurjchem-20 11 53     SPACE eurjchem-20 11 54 dna dna PROPN eurjchem-20 11 55     SPACE eurjchem-20 11 56 chain chain NOUN eurjchem-20 11 57     SPACE eurjchem-20 12 1 [ [ X eurjchem-20 12 2 3‐5 3‐5 NUM eurjchem-20 12 3 ] ] X eurjchem-20 12 4 . . PUNCT eurjchem-20 12 5     SPACE eurjchem-20 13 1 the the DET eurjchem-20 13 2     SPACE eurjchem-20 13 3 efficiency efficiency NOUN eurjchem-20 13 4     SPACE eurjchem-20 13 5 of of ADP eurjchem-20 13 6     SPACE eurjchem-20 13 7 this this DET eurjchem-20 13 8     SPACE eurjchem-20 13 9 phosphorylation phosphorylation NOUN eurjchem-20 13 10     SPACE eurjchem-20 13 11 process process NOUN eurjchem-20 13 12     SPACE eurjchem-20 13 13 is be AUX eurjchem-20 13 14     SPACE eurjchem-20 13 15 extremely extremely ADV eurjchem-20 13 16     SPACE eurjchem-20 13 17 slow slow ADJ eurjchem-20 13 18 . . PUNCT eurjchem-20 13 19     SPACE eurjchem-20 14 1 therefore therefore ADV eurjchem-20 14 2 , , PUNCT eurjchem-20 14 3     SPACE eurjchem-20 14 4 many many ADJ eurjchem-20 14 5     SPACE eurjchem-20 14 6 efforts effort NOUN eurjchem-20 14 7     SPACE eurjchem-20 14 8 have have AUX eurjchem-20 14 9     SPACE eurjchem-20 14 10 been be AUX eurjchem-20 14 11     SPACE eurjchem-20 14 12 made make VERB eurjchem-20 14 13     SPACE eurjchem-20 14 14 to to PART eurjchem-20 14 15     SPACE eurjchem-20 14 16 improve improve VERB eurjchem-20 14 17     SPACE eurjchem-20 14 18 therapeutic therapeutic ADJ eurjchem-20 14 19     SPACE eurjchem-20 14 20 properties property NOUN eurjchem-20 14 21     SPACE eurjchem-20 14 22 by by ADP eurjchem-20 14 23     SPACE eurjchem-20 14 24 taking taking NOUN eurjchem-20 14 25     SPACE eurjchem-20 14 26 at at ADP eurjchem-20 14 27     SPACE eurjchem-20 14 28 least least ADJ eurjchem-20 14 29     SPACE eurjchem-20 14 30 the the DET eurjchem-20 14 31     SPACE eurjchem-20 14 32 first first ADJ eurjchem-20 14 33     SPACE eurjchem-20 14 34 phosphorylation phosphorylation NOUN eurjchem-20 14 35     SPACE eurjchem-20 14 36 step step NOUN eurjchem-20 14 37 . . PUNCT eurjchem-20 14 38     SPACE eurjchem-20 15 1 this this DET eurjchem-20 15 2     SPACE eurjchem-20 15 3 approach approach NOUN eurjchem-20 15 4     SPACE eurjchem-20 15 5 has have AUX eurjchem-20 15 6     SPACE eurjchem-20 15 7 resulted result VERB eurjchem-20 15 8     SPACE eurjchem-20 15 9 in in ADP eurjchem-20 15 10     SPACE eurjchem-20 15 11 the the DET eurjchem-20 15 12     SPACE eurjchem-20 15 13 synthesis synthesis NOUN eurjchem-20 15 14     SPACE eurjchem-20 15 15 of of ADP eurjchem-20 15 16     SPACE eurjchem-20 15 17 potential potential ADJ eurjchem-20 15 18     SPACE eurjchem-20 15 19 numerous numerous ADJ eurjchem-20 15 20     SPACE eurjchem-20 15 21 nucleotide nucleotide NOUN eurjchem-20 15 22     SPACE eurjchem-20 15 23 analogues analogue NOUN eurjchem-20 15 24     SPACE eurjchem-20 15 25 as as ADP eurjchem-20 15 26     SPACE eurjchem-20 15 27 drugs drug NOUN eurjchem-20 15 28     SPACE eurjchem-20 16 1 [ [ X eurjchem-20 16 2 6‐10 6‐10 NUM eurjchem-20 16 3 ] ] PUNCT eurjchem-20 16 4 . . PUNCT eurjchem-20 16 5     SPACE eurjchem-20 17 1 these these DET eurjchem-20 17 2     SPACE eurjchem-20 17 3 potent potent ADJ eurjchem-20 17 4     SPACE eurjchem-20 17 5 biological biological ADJ eurjchem-20 17 6     SPACE eurjchem-20 17 7 activities activity NOUN eurjchem-20 17 8     SPACE eurjchem-20 17 9 of of ADP eurjchem-20 17 10     SPACE eurjchem-20 17 11 stavudine stavudine NOUN eurjchem-20 17 12     SPACE eurjchem-20 17 13 have have AUX eurjchem-20 17 14     SPACE eurjchem-20 17 15 stimulated stimulate VERB eurjchem-20 17 16     SPACE eurjchem-20 17 17 great great ADJ eurjchem-20 17 18     SPACE eurjchem-20 17 19 interest interest NOUN eurjchem-20 17 20     SPACE eurjchem-20 17 21 in in ADP eurjchem-20 17 22     SPACE eurjchem-20 17 23 the the DET eurjchem-20 17 24     SPACE eurjchem-20 17 25 synthesis synthesis NOUN eurjchem-20 17 26     SPACE eurjchem-20 17 27 of of ADP eurjchem-20 17 28     SPACE eurjchem-20 17 29 phosphorylated phosphorylate VERB eurjchem-20 17 30     SPACE eurjchem-20 17 31 compounds compound NOUN eurjchem-20 17 32     SPACE eurjchem-20 17 33 for for ADP eurjchem-20 17 34     SPACE eurjchem-20 17 35 extensive extensive ADJ eurjchem-20 17 36     SPACE eurjchem-20 17 37 studies study NOUN eurjchem-20 17 38     SPACE eurjchem-20 17 39 related relate VERB eurjchem-20 17 40     SPACE eurjchem-20 17 41 to to ADP eurjchem-20 17 42     SPACE eurjchem-20 17 43 their their PRON eurjchem-20 17 44     SPACE eurjchem-20 17 45 biological biological ADJ eurjchem-20 17 46     SPACE eurjchem-20 17 47 activities activity NOUN eurjchem-20 17 48 . . PUNCT eurjchem-20 17 49     SPACE eurjchem-20 18 1 in in ADP eurjchem-20 18 2     SPACE eurjchem-20 18 3 view view NOUN eurjchem-20 18 4     SPACE eurjchem-20 18 5 of of ADP eurjchem-20 18 6     SPACE eurjchem-20 18 7 these these PRON eurjchem-20 18 8 , , PUNCT eurjchem-20 18 9     SPACE eurjchem-20 18 10 we we PRON eurjchem-20 18 11     SPACE eurjchem-20 18 12 have have AUX eurjchem-20 18 13     SPACE eurjchem-20 18 14 focused focus VERB eurjchem-20 18 15     SPACE eurjchem-20 18 16 on on ADP eurjchem-20 18 17     SPACE eurjchem-20 18 18 the the DET eurjchem-20 18 19     SPACE eurjchem-20 18 20 synthesis synthesis NOUN eurjchem-20 18 21     SPACE eurjchem-20 18 22 of of ADP eurjchem-20 18 23     SPACE eurjchem-20 18 24 a a DET eurjchem-20 18 25     SPACE eurjchem-20 18 26 series series NOUN eurjchem-20 18 27     SPACE eurjchem-20 18 28 of of ADP eurjchem-20 18 29     SPACE eurjchem-20 18 30 novel novel NOUN eurjchem-20 18 31     SPACE eurjchem-20 18 32 phosphorylated phosphorylate VERB eurjchem-20 18 33     SPACE eurjchem-20 18 34 derivatives derivative NOUN eurjchem-20 18 35     SPACE eurjchem-20 18 36 of of ADP eurjchem-20 18 37     SPACE eurjchem-20 18 38 stavudine stavudine NOUN eurjchem-20 18 39     SPACE eurjchem-20 18 40 with with ADP eurjchem-20 18 41     SPACE eurjchem-20 18 42 several several ADJ eurjchem-20 18 43     SPACE eurjchem-20 18 44 bioactive bioactive NOUN eurjchem-20 18 45     SPACE eurjchem-20 18 46 groups group NOUN eurjchem-20 18 47     SPACE eurjchem-20 18 48 at at ADP eurjchem-20 18 49     SPACE eurjchem-20 18 50 the the DET eurjchem-20 18 51     SPACE eurjchem-20 18 52 phosphorus phosphorus NOUN eurjchem-20 18 53     SPACE eurjchem-20 18 54 and and CCONJ eurjchem-20 18 55     SPACE eurjchem-20 18 56 evaluated evaluated ADJ eurjchem-20 18 57     SPACE eurjchem-20 18 58 antioxidant antioxidant NOUN eurjchem-20 18 59     SPACE eurjchem-20 18 60 and and CCONJ eurjchem-20 18 61     SPACE eurjchem-20 18 62 antibacterial antibacterial ADJ eurjchem-20 18 63     SPACE eurjchem-20 18 64 properties property NOUN eurjchem-20 18 65 . . PUNCT eurjchem-20 18 66     SPACE eurjchem-20 19 1 the the DET eurjchem-20 19 2     SPACE eurjchem-20 19 3 oxidative oxidative ADJ eurjchem-20 19 4     SPACE eurjchem-20 19 5 stress stress NOUN eurjchem-20 19 6     SPACE eurjchem-20 19 7 of of ADP eurjchem-20 19 8     SPACE eurjchem-20 19 9 stavudine stavudine ADJ eurjchem-20 19 10     SPACE eurjchem-20 19 11 derivatives derivative NOUN eurjchem-20 19 12     SPACE eurjchem-20 19 13 was be AUX eurjchem-20 19 14     SPACE eurjchem-20 19 15 assessed assess VERB eurjchem-20 19 16     SPACE eurjchem-20 19 17 by by ADP eurjchem-20 19 18     SPACE eurjchem-20 19 19 estimating estimate VERB eurjchem-20 19 20     SPACE eurjchem-20 19 21 their their PRON eurjchem-20 19 22     SPACE eurjchem-20 19 23 activities activity NOUN eurjchem-20 19 24     SPACE eurjchem-20 19 25 on on ADP eurjchem-20 19 26     SPACE eurjchem-20 19 27 dpph dpph AUX eurjchem-20 19 28     SPACE eurjchem-20 19 29 using use VERB eurjchem-20 19 30     SPACE eurjchem-20 19 31 natural natural ADJ eurjchem-20 19 32     SPACE eurjchem-20 19 33 antioxidant antioxidant NOUN eurjchem-20 19 34     SPACE eurjchem-20 19 35 vitamin vitamin NOUN eurjchem-20 19 36     SPACE eurjchem-20 19 37 c c NOUN eurjchem-20 19 38     SPACE eurjchem-20 19 39 as as ADP eurjchem-20 19 40     SPACE eurjchem-20 19 41 standard standard NOUN eurjchem-20 19 42 . . PUNCT eurjchem-20 19 43     SPACE eurjchem-20 19 44 antibacterial antibacterial ADJ eurjchem-20 19 45     SPACE eurjchem-20 19 46 activity activity NOUN eurjchem-20 19 47     SPACE eurjchem-20 19 48 was be AUX eurjchem-20 19 49     SPACE eurjchem-20 19 50 investigated investigate VERB eurjchem-20 19 51     SPACE eurjchem-20 19 52 against against ADP eurjchem-20 19 53     SPACE eurjchem-20 19 54 gram gram NOUN eurjchem-20 19 55     SPACE eurjchem-20 19 56 positive positive ADJ eurjchem-20 19 57     SPACE eurjchem-20 19 58 bacteria bacteria NOUN eurjchem-20 19 59 : : PUNCT eurjchem-20 19 60     SPACE eurjchem-20 19 61 bacillus bacillus NOUN eurjchem-20 19 62     SPACE eurjchem-20 19 63 subtilis subtili NOUN eurjchem-20 19 64 , , PUNCT eurjchem-20 19 65     SPACE eurjchem-20 19 66 staphylococcus staphylococcus NOUN eurjchem-20 19 67     SPACE eurjchem-20 19 68 aureus aureus NOUN eurjchem-20 19 69     SPACE eurjchem-20 19 70 and and CCONJ eurjchem-20 19 71     SPACE eurjchem-20 19 72 gram gram NOUN eurjchem-20 19 73     SPACE eurjchem-20 19 74 negative negative ADJ eurjchem-20 19 75     SPACE eurjchem-20 19 76 bacteria bacteria NOUN eurjchem-20 19 77 : : PUNCT eurjchem-20 19 78     SPACE eurjchem-20 19 79 escherichia escherichia NOUN eurjchem-20 19 80     SPACE eurjchem-20 19 81 coli coli NOUN eurjchem-20 19 82     SPACE eurjchem-20 19 83 and and CCONJ eurjchem-20 19 84     SPACE eurjchem-20 19 85 klebsiella klebsiella NOUN eurjchem-20 19 86     SPACE eurjchem-20 19 87 pneumoniae pneumoniae NOUN eurjchem-20 19 88 . . PUNCT eurjchem-20 19 89     SPACE eurjchem-20 20 1 the the DET eurjchem-20 20 2     SPACE eurjchem-20 20 3 structures structure NOUN eurjchem-20 20 4     SPACE eurjchem-20 20 5 of of ADP eurjchem-20 20 6     SPACE eurjchem-20 20 7 all all PRON eurjchem-20 20 8     SPACE eurjchem-20 20 9 the the DET eurjchem-20 20 10     SPACE eurjchem-20 20 11 newly newly ADV eurjchem-20 20 12     SPACE eurjchem-20 20 13 synthesized synthesize VERB eurjchem-20 20 14     SPACE eurjchem-20 20 15 compounds compound VERB eurjchem-20 20 16     SPACE eurjchem-20 20 17 4a­l 4a­l NOUN eurjchem-20 20 18     SPACE eurjchem-20 20 19 have have AUX eurjchem-20 20 20     SPACE eurjchem-20 20 21 been be AUX eurjchem-20 20 22     SPACE eurjchem-20 20 23 established establish VERB eurjchem-20 20 24     SPACE eurjchem-20 20 25 by by ADP eurjchem-20 20 26     SPACE eurjchem-20 20 27 elemental elemental NOUN eurjchem-20 20 28     SPACE eurjchem-20 20 29 analyses analysis NOUN eurjchem-20 20 30     SPACE eurjchem-20 20 31 and and CCONJ eurjchem-20 20 32     SPACE eurjchem-20 20 33 spectral spectral ADJ eurjchem-20 20 34     SPACE eurjchem-20 20 35 data data PROPN eurjchem-20 20 36     SPACE eurjchem-20 20 37 ( ( PUNCT eurjchem-20 20 38 ir ir PROPN eurjchem-20 20 39 , , PUNCT eurjchem-20 20 40     SPACE eurjchem-20 20 41 1h 1h NUM eurjchem-20 20 42 , , PUNCT eurjchem-20 20 43     SPACE eurjchem-20 20 44 13c 13c NOUN eurjchem-20 20 45 , , PUNCT eurjchem-20 20 46     SPACE eurjchem-20 20 47 31p 31p NUM eurjchem-20 20 48     SPACE eurjchem-20 20 49 nmr nmr NOUN eurjchem-20 20 50     SPACE eurjchem-20 20 51 and and CCONJ eurjchem-20 20 52     SPACE eurjchem-20 20 53 ms ms NOUN eurjchem-20 20 54 ) ) PUNCT eurjchem-20 20 55 . . PUNCT eurjchem-20 20 56         SPACE eurjchem-20 21 1 2 2 NUM eurjchem-20 21 2 . . PUNCT eurjchem-20 21 3     SPACE eurjchem-20 21 4 experimental experimental ADJ eurjchem-20 21 5         SPACE eurjchem-20 21 6 2.1 2.1 NUM eurjchem-20 21 7 . . PUNCT eurjchem-20 21 8     SPACE eurjchem-20 21 9 instrumentation instrumentation NOUN eurjchem-20 21 10         SPACE eurjchem-20 21 11 sigma‐aldrich sigma‐aldrich PROPN eurjchem-20 21 12 , , PUNCT eurjchem-20 21 13     SPACE eurjchem-20 21 14 merck merck NOUN eurjchem-20 21 15     SPACE eurjchem-20 21 16 and and CCONJ eurjchem-20 21 17     SPACE eurjchem-20 21 18 lancaster lancaster NOUN eurjchem-20 21 19     SPACE eurjchem-20 21 20 chemicals chemical NOUN eurjchem-20 21 21     SPACE eurjchem-20 21 22 were be AUX eurjchem-20 21 23     SPACE eurjchem-20 21 24 used use VERB eurjchem-20 21 25     SPACE eurjchem-20 21 26 as as ADP eurjchem-20 21 27     SPACE eurjchem-20 21 28 such such ADJ eurjchem-20 21 29     SPACE eurjchem-20 21 30 without without ADP eurjchem-20 21 31     SPACE eurjchem-20 21 32 further further ADJ eurjchem-20 21 33     SPACE eurjchem-20 21 34 purification purification NOUN eurjchem-20 21 35 . . PUNCT eurjchem-20 21 36     SPACE eurjchem-20 22 1 all all DET eurjchem-20 22 2     SPACE eurjchem-20 22 3 solvents solvent NOUN eurjchem-20 22 4     SPACE eurjchem-20 22 5 used use VERB eurjchem-20 22 6     SPACE eurjchem-20 22 7 for for ADP eurjchem-20 22 8     SPACE eurjchem-20 22 9 spectroscopic spectroscopic NOUN eurjchem-20 22 10     SPACE eurjchem-20 22 11 and and CCONJ eurjchem-20 22 12     SPACE eurjchem-20 22 13 other other ADJ eurjchem-20 22 14     SPACE eurjchem-20 22 15 physical physical ADJ eurjchem-20 22 16     SPACE eurjchem-20 22 17 studies study NOUN eurjchem-20 22 18     SPACE eurjchem-20 22 19 were be AUX eurjchem-20 22 20     SPACE eurjchem-20 22 21 reagent reagent ADJ eurjchem-20 22 22     SPACE eurjchem-20 22 23 grade grade NOUN eurjchem-20 22 24     SPACE eurjchem-20 22 25 and and CCONJ eurjchem-20 22 26     SPACE eurjchem-20 22 27 were be AUX eurjchem-20 22 28     SPACE eurjchem-20 22 29 further far ADV eurjchem-20 22 30     SPACE eurjchem-20 22 31 purified purify VERB eurjchem-20 22 32     SPACE eurjchem-20 22 33 by by ADP eurjchem-20 22 34     SPACE eurjchem-20 22 35 literature literature NOUN eurjchem-20 22 36     SPACE eurjchem-20 22 37 methods method NOUN eurjchem-20 22 38     SPACE eurjchem-20 23 1 [ [ X eurjchem-20 23 2 11 11 NUM eurjchem-20 23 3 ] ] PUNCT eurjchem-20 23 4 . . PUNCT eurjchem-20 23 5     SPACE eurjchem-20 23 6 melting melt VERB eurjchem-20 23 7     SPACE eurjchem-20 23 8 points point NOUN eurjchem-20 23 9     SPACE eurjchem-20 23 10 were be AUX eurjchem-20 23 11     SPACE eurjchem-20 23 12 determined determine VERB eurjchem-20 23 13     SPACE eurjchem-20 23 14 by by ADP eurjchem-20 23 15     SPACE eurjchem-20 23 16 guna guna PROPN eurjchem-20 23 17     SPACE eurjchem-20 23 18 digital digital PROPN eurjchem-20 23 19     SPACE eurjchem-20 23 20 melting melting NOUN eurjchem-20 23 21     SPACE eurjchem-20 23 22 point point NOUN eurjchem-20 23 23     SPACE eurjchem-20 23 24 apparatus apparatus NOUN eurjchem-20 23 25     SPACE eurjchem-20 23 26 using use VERB eurjchem-20 23 27     SPACE eurjchem-20 23 28 a a DET eurjchem-20 23 29     SPACE eurjchem-20 23 30 calibrated calibrate VERB eurjchem-20 23 31     SPACE eurjchem-20 23 32 centigrade centigrade NOUN eurjchem-20 23 33     SPACE eurjchem-20 23 34 thermometer thermometer NOUN eurjchem-20 23 35 . . PUNCT eurjchem-20 23 36     SPACE eurjchem-20 24 1 ir ir PROPN eurjchem-20 24 2     SPACE eurjchem-20 24 3 spectra spectra NOUN eurjchem-20 24 4     SPACE eurjchem-20 24 5 were be AUX eurjchem-20 24 6     SPACE eurjchem-20 24 7 recorded record VERB eurjchem-20 24 8     SPACE eurjchem-20 24 9 in in ADP eurjchem-20 24 10     SPACE eurjchem-20 24 11 kbr kbr PROPN eurjchem-20 24 12     SPACE eurjchem-20 24 13 disks disk NOUN eurjchem-20 24 14     SPACE eurjchem-20 24 15 on on ADP eurjchem-20 24 16     SPACE eurjchem-20 24 17 a a DET eurjchem-20 24 18     SPACE eurjchem-20 24 19 perkin‐elmer perkin‐elmer NOUN eurjchem-20 24 20     SPACE eurjchem-20 24 21 model model NOUN eurjchem-20 24 22     SPACE eurjchem-20 24 23 281‐b 281‐b NUM eurjchem-20 24 24     SPACE eurjchem-20 24 25 spectrophotometer spectrophotometer NOUN eurjchem-20 24 26     SPACE eurjchem-20 24 27 in in ADP eurjchem-20 24 28     SPACE eurjchem-20 24 29 wave wave NOUN eurjchem-20 24 30     SPACE eurjchem-20 24 31 numbers number NOUN eurjchem-20 24 32     SPACE eurjchem-20 24 33 ( ( PUNCT eurjchem-20 24 34 cm‐1 cm‐1 NOUN eurjchem-20 24 35 ) ) PUNCT eurjchem-20 24 36 . . PUNCT eurjchem-20 24 37     SPACE eurjchem-20 25 1 1h 1h NUM eurjchem-20 25 2 , , PUNCT eurjchem-20 25 3     SPACE eurjchem-20 25 4 13c 13c NOUN eurjchem-20 25 5     SPACE eurjchem-20 25 6 and and CCONJ eurjchem-20 25 7     SPACE eurjchem-20 25 8 31p 31p NOUN eurjchem-20 25 9     SPACE eurjchem-20 25 10 nmr nmr NOUN eurjchem-20 25 11     SPACE eurjchem-20 25 12 spectra spectra NOUN eurjchem-20 25 13     SPACE eurjchem-20 25 14 were be AUX eurjchem-20 25 15     SPACE eurjchem-20 25 16 recorded record VERB eurjchem-20 25 17     SPACE eurjchem-20 25 18 as as ADP eurjchem-20 25 19     SPACE eurjchem-20 25 20 solutions solution NOUN eurjchem-20 25 21     SPACE eurjchem-20 25 22 in in ADP eurjchem-20 25 23     SPACE eurjchem-20 25 24 dmso‐d6 dmso‐d6 NOUN eurjchem-20 25 25     SPACE eurjchem-20 25 26 on on ADP eurjchem-20 25 27     SPACE eurjchem-20 25 28 a a DET eurjchem-20 25 29     SPACE eurjchem-20 25 30 bruker bruker NOUN eurjchem-20 25 31     SPACE eurjchem-20 25 32 avance avance PROPN eurjchem-20 25 33     SPACE eurjchem-20 25 34 iii iii NOUN eurjchem-20 25 35     SPACE eurjchem-20 25 36 500 500 NUM eurjchem-20 25 37     SPACE eurjchem-20 25 38 mhz mhz NOUN eurjchem-20 25 39     SPACE eurjchem-20 25 40 spectrometer spectrometer NOUN eurjchem-20 25 41     SPACE eurjchem-20 25 42 operating operating NOUN eurjchem-20 25 43     SPACE eurjchem-20 25 44 at at ADP eurjchem-20 25 45     SPACE eurjchem-20 25 46 500 500 NUM eurjchem-20 25 47     SPACE eurjchem-20 25 48 mhz mhz NOUN eurjchem-20 25 49     SPACE eurjchem-20 25 50 for for ADP eurjchem-20 25 51     SPACE eurjchem-20 25 52 1h 1h NUM eurjchem-20 25 53 , , PUNCT eurjchem-20 25 54     SPACE eurjchem-20 25 55 125 125 NUM eurjchem-20 25 56     SPACE eurjchem-20 25 57 mhz mhz NOUN eurjchem-20 25 58     SPACE eurjchem-20 25 59 for for ADP eurjchem-20 25 60     SPACE eurjchem-20 25 61 13c 13c NOUN eurjchem-20 25 62     SPACE eurjchem-20 25 63 and and CCONJ eurjchem-20 25 64     SPACE eurjchem-20 25 65 202.4 202.4 NUM eurjchem-20 25 66     SPACE eurjchem-20 25 67 mhz mhz NOUN eurjchem-20 25 68     SPACE eurjchem-20 25 69 for for ADP eurjchem-20 25 70     SPACE eurjchem-20 25 71 31p 31p NOUN eurjchem-20 25 72     SPACE eurjchem-20 25 73 nuclei nucleus NOUN eurjchem-20 25 74     SPACE eurjchem-20 25 75 and and CCONJ eurjchem-20 25 76     SPACE eurjchem-20 25 77 their their PRON eurjchem-20 25 78     SPACE eurjchem-20 25 79 chemical chemical NOUN eurjchem-20 25 80     SPACE eurjchem-20 25 81 shifts shift NOUN eurjchem-20 25 82     SPACE eurjchem-20 25 83 were be AUX eurjchem-20 25 84     SPACE eurjchem-20 25 85 expressed express VERB eurjchem-20 25 86     SPACE eurjchem-20 25 87 in in ADP eurjchem-20 25 88     SPACE eurjchem-20 25 89 ppm ppm NOUN eurjchem-20 25 90     SPACE eurjchem-20 25 91 with with ADP eurjchem-20 25 92     SPACE eurjchem-20 25 93 reference reference NOUN eurjchem-20 25 94     SPACE eurjchem-20 25 95 to to PART eurjchem-20 25 96     SPACE eurjchem-20 25 97 tetramethylsilane tetramethylsilane VERB eurjchem-20 25 98     SPACE eurjchem-20 25 99 and and CCONJ eurjchem-20 25 100     SPACE eurjchem-20 25 101 85 85 NUM eurjchem-20 25 102     SPACE eurjchem-20 25 103 % % NOUN eurjchem-20 25 104     SPACE eurjchem-20 25 105 h3po4 h3po4 NOUN eurjchem-20 25 106     SPACE eurjchem-20 25 107 respectively respectively ADV eurjchem-20 25 108 . . PUNCT eurjchem-20 25 109     SPACE eurjchem-20 25 110 mass mass PROPN eurjchem-20 25 111     SPACE eurjchem-20 25 112 spectra spectra NOUN eurjchem-20 25 113     SPACE eurjchem-20 25 114 were be AUX eurjchem-20 25 115     SPACE eurjchem-20 25 116 recorded record VERB eurjchem-20 25 117     SPACE eurjchem-20 25 118 on on ADP eurjchem-20 25 119     SPACE eurjchem-20 25 120 a a DET eurjchem-20 25 121     SPACE eurjchem-20 25 122 jeol jeol NOUN eurjchem-20 25 123     SPACE eurjchem-20 25 124 gcmate gcmate NOUN eurjchem-20 25 125     SPACE eurjchem-20 25 126 ii ii NOUN eurjchem-20 25 127     SPACE eurjchem-20 25 128 mass mass PROPN eurjchem-20 25 129     SPACE eurjchem-20 25 130 spectrometer spectrometer NOUN eurjchem-20 25 131 . . PUNCT eurjchem-20 25 132     SPACE eurjchem-20 26 1 elemental elemental NOUN eurjchem-20 26 2     SPACE eurjchem-20 26 3 analyses analysis NOUN eurjchem-20 26 4     SPACE eurjchem-20 26 5 were be AUX eurjchem-20 26 6     SPACE eurjchem-20 26 7 performed perform VERB eurjchem-20 26 8     SPACE eurjchem-20 26 9 by by ADP eurjchem-20 26 10     SPACE eurjchem-20 26 11 central central ADJ eurjchem-20 26 12     SPACE eurjchem-20 26 13 drug drug NOUN eurjchem-20 26 14     SPACE eurjchem-20 26 15 research research NOUN eurjchem-20 26 16     SPACE eurjchem-20 26 17 institute institute PROPN eurjchem-20 26 18 , , PUNCT eurjchem-20 26 19     SPACE eurjchem-20 26 20 lucknow lucknow PROPN eurjchem-20 26 21 , , PUNCT eurjchem-20 26 22     SPACE eurjchem-20 26 23 india india PROPN eurjchem-20 26 24 . . PUNCT eurjchem-20 26 25         SPACE eurjchem-20 27 1 2.2 2.2 NUM eurjchem-20 27 2 . . PUNCT eurjchem-20 27 3     SPACE eurjchem-20 27 4 synthesis synthesis NOUN eurjchem-20 27 5         SPACE eurjchem-20 27 6 a a DET eurjchem-20 27 7     SPACE eurjchem-20 27 8 solution solution NOUN eurjchem-20 27 9     SPACE eurjchem-20 27 10 of of ADP eurjchem-20 27 11     SPACE eurjchem-20 27 12 various various ADJ eurjchem-20 27 13     SPACE eurjchem-20 27 14 cyclicamines cyclicamine NOUN eurjchem-20 27 15         SPACE eurjchem-20 27 16 and and CCONJ eurjchem-20 27 17     SPACE eurjchem-20 27 18 amino amino NOUN eurjchem-20 27 19     SPACE eurjchem-20 27 20 acid acid NOUN eurjchem-20 27 21     SPACE eurjchem-20 27 22 esters ester NOUN eurjchem-20 27 23     SPACE eurjchem-20 27 24 ( ( PUNCT eurjchem-20 27 25 0.002 0.002 NUM eurjchem-20 27 26     SPACE eurjchem-20 27 27 mole mole NOUN eurjchem-20 27 28 ) ) PUNCT eurjchem-20 27 29 , , PUNCT eurjchem-20 27 30         SPACE eurjchem-20 27 31 in in ADP eurjchem-20 27 32     SPACE eurjchem-20 27 33 dry dry ADJ eurjchem-20 27 34     SPACE eurjchem-20 27 35 tetrahydrofuran tetrahydrofuran NOUN eurjchem-20 27 36     SPACE eurjchem-20 27 37 ( ( PUNCT eurjchem-20 27 38 thf thf NOUN eurjchem-20 27 39 ) ) PUNCT eurjchem-20 27 40     SPACE eurjchem-20 27 41 ( ( PUNCT eurjchem-20 27 42 10 10 NUM eurjchem-20 27 43     SPACE eurjchem-20 27 44 ml ml NOUN eurjchem-20 27 45 ) ) PUNCT eurjchem-20 27 46     SPACE eurjchem-20 27 47 and and CCONJ eurjchem-20 27 48     SPACE eurjchem-20 27 49 triethylamine triethylamine NOUN eurjchem-20 27 50     SPACE eurjchem-20 27 51 ( ( PUNCT eurjchem-20 27 52 tea tea NOUN eurjchem-20 27 53 ) ) PUNCT eurjchem-20 27 54     SPACE eurjchem-20 27 55 ( ( PUNCT eurjchem-20 27 56 0.002 0.002 NUM eurjchem-20 27 57     SPACE eurjchem-20 27 58 mole mole NOUN eurjchem-20 27 59 ) ) PUNCT eurjchem-20 27 60 , , PUNCT eurjchem-20 27 61     SPACE eurjchem-20 27 62 was be AUX eurjchem-20 27 63     SPACE eurjchem-20 27 64 added add VERB eurjchem-20 27 65     SPACE eurjchem-20 27 66 dropwise dropwise NOUN eurjchem-20 27 67     SPACE eurjchem-20 27 68 over over ADP eurjchem-20 27 69     SPACE eurjchem-20 27 70 a a DET eurjchem-20 27 71     SPACE eurjchem-20 27 72 period period NOUN eurjchem-20 27 73     SPACE eurjchem-20 27 74 of of ADP eurjchem-20 27 75     SPACE eurjchem-20 27 76 15 15 NUM eurjchem-20 27 77     SPACE eurjchem-20 27 78 minutes minute NOUN eurjchem-20 27 79     SPACE eurjchem-20 27 80 to to ADP eurjchem-20 27 81     SPACE eurjchem-20 27 82 a a DET eurjchem-20 27 83     SPACE eurjchem-20 27 84 stirred stir VERB eurjchem-20 27 85     SPACE eurjchem-20 27 86 solution solution NOUN eurjchem-20 27 87     SPACE eurjchem-20 27 88 of of ADP eurjchem-20 27 89     SPACE eurjchem-20 27 90 bis(2‐ bis(2‐ PROPN eurjchem-20 27 91 chloroethyl)phosphoramidicdichloride/4‐nitro chloroethyl)phosphoramidicdichloride/4‐nitro PROPN eurjchem-20 27 92     SPACE eurjchem-20 27 93 phenylphos phenylphos NOUN eurjchem-20 27 94     SPACE eurjchem-20 27 95 phorodichloridate phorodichloridate NOUN eurjchem-20 27 96     SPACE eurjchem-20 27 97 ( ( PUNCT eurjchem-20 27 98 0.002 0.002 NUM eurjchem-20 27 99     SPACE eurjchem-20 27 100 mole mole NOUN eurjchem-20 27 101 ) ) PUNCT eurjchem-20 27 102     SPACE eurjchem-20 27 103 in in ADP eurjchem-20 27 104     SPACE eurjchem-20 27 105 20 20 NUM eurjchem-20 27 106     SPACE eurjchem-20 27 107 ml ml NOUN eurjchem-20 27 108     SPACE eurjchem-20 27 109 of of ADP eurjchem-20 27 110         SPACE eurjchem-20 27 111 thf thf NOUN eurjchem-20 27 112     SPACE eurjchem-20 27 113 at at ADP eurjchem-20 27 114     SPACE eurjchem-20 27 115 ‐10‐0 ‐10‐0 NOUN eurjchem-20 27 116     SPACE eurjchem-20 27 117 oc oc AUX eurjchem-20 27 118     SPACE eurjchem-20 27 119 ( ( PUNCT eurjchem-20 27 120 scheme scheme NOUN eurjchem-20 27 121     SPACE eurjchem-20 27 122 1 1 NUM eurjchem-20 27 123 ) ) PUNCT eurjchem-20 27 124 . . PUNCT eurjchem-20 27 125       SPACE eurjchem-20 28 1 298 298 NUM eurjchem-20 28 2     SPACE eurjchem-20 28 3 rao rao PROPN eurjchem-20 28 4     SPACE eurjchem-20 28 5 et et PROPN eurjchem-20 28 6     SPACE eurjchem-20 28 7 al al PROPN eurjchem-20 28 8 . . PROPN eurjchem-20 28 9     SPACE eurjchem-20 28 10 / / SYM eurjchem-20 28 11     SPACE eurjchem-20 28 12 european european ADJ eurjchem-20 28 13     SPACE eurjchem-20 28 14 journal journal NOUN eurjchem-20 28 15     SPACE eurjchem-20 28 16 of of ADP eurjchem-20 28 17     SPACE eurjchem-20 28 18 chemistry chemistry NOUN eurjchem-20 28 19     SPACE eurjchem-20 28 20 1 1 NUM eurjchem-20 28 21     SPACE eurjchem-20 28 22 ( ( PUNCT eurjchem-20 28 23 4 4 NUM eurjchem-20 28 24 ) ) PUNCT eurjchem-20 28 25     SPACE eurjchem-20 28 26 ( ( PUNCT eurjchem-20 28 27 2010 2010 NUM eurjchem-20 28 28 ) ) PUNCT eurjchem-20 28 29     SPACE eurjchem-20 29 1 297­301 297­301 NUM eurjchem-20 29 2                     SPACE eurjchem-20 29 3 scheme scheme NOUN eurjchem-20 29 4     SPACE eurjchem-20 29 5 1 1 NUM eurjchem-20 29 6             SPACE eurjchem-20 29 7 after after ADP eurjchem-20 29 8     SPACE eurjchem-20 29 9 stirring stirring NOUN eurjchem-20 29 10     SPACE eurjchem-20 29 11 for for ADP eurjchem-20 29 12     SPACE eurjchem-20 29 13 2 2 NUM eurjchem-20 29 14     SPACE eurjchem-20 29 15 hours hour NOUN eurjchem-20 29 16 , , PUNCT eurjchem-20 29 17     SPACE eurjchem-20 29 18 formation formation NOUN eurjchem-20 29 19     SPACE eurjchem-20 29 20 of of ADP eurjchem-20 29 21     SPACE eurjchem-20 29 22 intermediate intermediate ADJ eurjchem-20 29 23     SPACE eurjchem-20 29 24 monochlorides monochloride NOUN eurjchem-20 29 25     SPACE eurjchem-20 29 26 2a­l 2a­l NOUN eurjchem-20 29 27     SPACE eurjchem-20 29 28 was be AUX eurjchem-20 29 29     SPACE eurjchem-20 29 30 ascertained ascertain VERB eurjchem-20 29 31     SPACE eurjchem-20 29 32 by by ADP eurjchem-20 29 33     SPACE eurjchem-20 29 34 thin thin ADJ eurjchem-20 29 35     SPACE eurjchem-20 29 36 layer layer NOUN eurjchem-20 29 37     SPACE eurjchem-20 29 38 chromatography chromatography NOUN eurjchem-20 29 39     SPACE eurjchem-20 29 40 performed perform VERB eurjchem-20 29 41     SPACE eurjchem-20 29 42 in in ADP eurjchem-20 29 43     SPACE eurjchem-20 29 44 7:3 7:3 NUM eurjchem-20 29 45     SPACE eurjchem-20 29 46 mixture mixture NOUN eurjchem-20 29 47     SPACE eurjchem-20 29 48 of of ADP eurjchem-20 29 49     SPACE eurjchem-20 29 50 ethyl ethyl PROPN eurjchem-20 29 51     SPACE eurjchem-20 29 52 acetate acetate NOUN eurjchem-20 29 53     SPACE eurjchem-20 29 54 and and CCONJ eurjchem-20 29 55     SPACE eurjchem-20 29 56 hexane hexane NOUN eurjchem-20 29 57 . . PUNCT eurjchem-20 29 58     SPACE eurjchem-20 29 59 to to ADP eurjchem-20 29 60     SPACE eurjchem-20 29 61 this this DET eurjchem-20 29 62     SPACE eurjchem-20 29 63 stavudine stavudine NOUN eurjchem-20 29 64     SPACE eurjchem-20 29 65 ( ( PUNCT eurjchem-20 29 66 0.002 0.002 NUM eurjchem-20 29 67     SPACE eurjchem-20 29 68 mole mole NOUN eurjchem-20 29 69 ) ) PUNCT eurjchem-20 29 70     SPACE eurjchem-20 29 71 in in ADP eurjchem-20 29 72     SPACE eurjchem-20 29 73 10 10 NUM eurjchem-20 29 74     SPACE eurjchem-20 29 75 ml ml NOUN eurjchem-20 29 76     SPACE eurjchem-20 29 77 of of ADP eurjchem-20 29 78     SPACE eurjchem-20 29 79 pyridine pyridine NOUN eurjchem-20 29 80     SPACE eurjchem-20 29 81 and and CCONJ eurjchem-20 29 82     SPACE eurjchem-20 29 83 tea tea NOUN eurjchem-20 29 84     SPACE eurjchem-20 29 85 ( ( PUNCT eurjchem-20 29 86 0.002 0.002 NUM eurjchem-20 29 87     SPACE eurjchem-20 29 88 mole mole NOUN eurjchem-20 29 89 ) ) PUNCT eurjchem-20 29 90 , , PUNCT eurjchem-20 29 91     SPACE eurjchem-20 29 92 was be AUX eurjchem-20 29 93     SPACE eurjchem-20 29 94 added add VERB eurjchem-20 29 95     SPACE eurjchem-20 29 96 dropwise dropwise NOUN eurjchem-20 29 97     SPACE eurjchem-20 29 98 at at ADP eurjchem-20 29 99     SPACE eurjchem-20 29 100 0 0 NUM eurjchem-20 29 101     SPACE eurjchem-20 29 102 ºc ºc PROPN eurjchem-20 29 103 . . PROPN eurjchem-20 29 104     SPACE eurjchem-20 29 105 after after ADP eurjchem-20 29 106     SPACE eurjchem-20 29 107 completion completion NOUN eurjchem-20 29 108     SPACE eurjchem-20 29 109 of of ADP eurjchem-20 29 110     SPACE eurjchem-20 29 111 the the DET eurjchem-20 29 112     SPACE eurjchem-20 29 113 addition addition NOUN eurjchem-20 29 114 , , PUNCT eurjchem-20 29 115     SPACE eurjchem-20 29 116 the the DET eurjchem-20 29 117     SPACE eurjchem-20 29 118 reaction reaction NOUN eurjchem-20 29 119     SPACE eurjchem-20 29 120 temperature temperature NOUN eurjchem-20 29 121     SPACE eurjchem-20 29 122 was be AUX eurjchem-20 29 123     SPACE eurjchem-20 29 124 slowly slowly ADV eurjchem-20 29 125     SPACE eurjchem-20 29 126 raised raise VERB eurjchem-20 29 127     SPACE eurjchem-20 29 128 to to ADP eurjchem-20 29 129     SPACE eurjchem-20 29 130 rt rt NOUN eurjchem-20 29 131     SPACE eurjchem-20 29 132 and and CCONJ eurjchem-20 29 133     SPACE eurjchem-20 29 134 continued continue VERB eurjchem-20 29 135     SPACE eurjchem-20 29 136 stirring stirring NOUN eurjchem-20 29 137     SPACE eurjchem-20 29 138 for for ADP eurjchem-20 29 139     SPACE eurjchem-20 29 140 an an DET eurjchem-20 29 141     SPACE eurjchem-20 29 142 additional additional ADJ eurjchem-20 29 143           SPACE eurjchem-20 29 144 10 10 NUM eurjchem-20 29 145     SPACE eurjchem-20 29 146 h. h. NOUN eurjchem-20 29 147     SPACE eurjchem-20 29 148 the the DET eurjchem-20 29 149     SPACE eurjchem-20 29 150 progress progress NOUN eurjchem-20 29 151     SPACE eurjchem-20 29 152 of of ADP eurjchem-20 29 153     SPACE eurjchem-20 29 154 the the DET eurjchem-20 29 155     SPACE eurjchem-20 29 156 reaction reaction NOUN eurjchem-20 29 157     SPACE eurjchem-20 29 158 was be AUX eurjchem-20 29 159     SPACE eurjchem-20 29 160 monitored monitor VERB eurjchem-20 29 161     SPACE eurjchem-20 29 162 by by ADP eurjchem-20 29 163     SPACE eurjchem-20 29 164 tlc tlc NOUN eurjchem-20 29 165     SPACE eurjchem-20 29 166 run run NOUN eurjchem-20 29 167     SPACE eurjchem-20 29 168 in in ADP eurjchem-20 29 169     SPACE eurjchem-20 29 170 9:1 9:1 NUM eurjchem-20 29 171     SPACE eurjchem-20 29 172 mixture mixture NOUN eurjchem-20 29 173     SPACE eurjchem-20 29 174 of of ADP eurjchem-20 29 175     SPACE eurjchem-20 29 176 ethylacetate ethylacetate VERB eurjchem-20 29 177     SPACE eurjchem-20 29 178 and and CCONJ eurjchem-20 29 179     SPACE eurjchem-20 29 180 hexane hexane NOUN eurjchem-20 29 181 . . PUNCT eurjchem-20 29 182     SPACE eurjchem-20 30 1 the the DET eurjchem-20 30 2     SPACE eurjchem-20 30 3 reaction reaction NOUN eurjchem-20 30 4     SPACE eurjchem-20 30 5 mixture mixture NOUN eurjchem-20 30 6     SPACE eurjchem-20 30 7 was be AUX eurjchem-20 30 8     SPACE eurjchem-20 30 9 filtered filter VERB eurjchem-20 30 10     SPACE eurjchem-20 30 11 to to PART eurjchem-20 30 12     SPACE eurjchem-20 30 13 remove remove VERB eurjchem-20 30 14     SPACE eurjchem-20 30 15 tea tea NOUN eurjchem-20 30 16     SPACE eurjchem-20 30 17 hydrochloride hydrochloride NOUN eurjchem-20 30 18     SPACE eurjchem-20 30 19 and and CCONJ eurjchem-20 30 20     SPACE eurjchem-20 30 21 the the DET eurjchem-20 30 22     SPACE eurjchem-20 30 23 solvent solvent NOUN eurjchem-20 30 24     SPACE eurjchem-20 30 25 in in ADP eurjchem-20 30 26     SPACE eurjchem-20 30 27 the the DET eurjchem-20 30 28     SPACE eurjchem-20 30 29 filtrate filtrate NOUN eurjchem-20 30 30     SPACE eurjchem-20 30 31 was be AUX eurjchem-20 30 32     SPACE eurjchem-20 30 33 removed remove VERB eurjchem-20 30 34     SPACE eurjchem-20 30 35 in in ADP eurjchem-20 30 36     SPACE eurjchem-20 30 37 a a DET eurjchem-20 30 38     SPACE eurjchem-20 30 39 rotaevaporator rotaevaporator NOUN eurjchem-20 30 40 . . PUNCT eurjchem-20 30 41     SPACE eurjchem-20 30 42 the the DET eurjchem-20 30 43     SPACE eurjchem-20 30 44 crude crude NOUN eurjchem-20 30 45     SPACE eurjchem-20 30 46 product product NOUN eurjchem-20 30 47     SPACE eurjchem-20 30 48 was be AUX eurjchem-20 30 49     SPACE eurjchem-20 30 50 purified purify VERB eurjchem-20 30 51     SPACE eurjchem-20 30 52 by by ADP eurjchem-20 30 53     SPACE eurjchem-20 30 54 column column NOUN eurjchem-20 30 55     SPACE eurjchem-20 30 56 chromatography chromatography NOUN eurjchem-20 30 57     SPACE eurjchem-20 30 58 on on ADP eurjchem-20 30 59     SPACE eurjchem-20 30 60 silica silica NOUN eurjchem-20 30 61     SPACE eurjchem-20 30 62 gel gel NOUN eurjchem-20 30 63     SPACE eurjchem-20 30 64 ( ( PUNCT eurjchem-20 30 65 60‐120 60‐120 NOUN eurjchem-20 30 66     SPACE eurjchem-20 30 67 mesh mesh NOUN eurjchem-20 30 68 ) ) PUNCT eurjchem-20 30 69     SPACE eurjchem-20 30 70 with with ADP eurjchem-20 30 71     SPACE eurjchem-20 30 72 chloroform chloroform NOUN eurjchem-20 30 73 : : PUNCT eurjchem-20 30 74     SPACE eurjchem-20 30 75 methanol methanol NOUN eurjchem-20 30 76     SPACE eurjchem-20 30 77 ( ( PUNCT eurjchem-20 30 78 9:1 9:1 NUM eurjchem-20 30 79 ) ) PUNCT eurjchem-20 30 80     SPACE eurjchem-20 30 81 as as ADP eurjchem-20 30 82     SPACE eurjchem-20 30 83 eluent eluent NOUN eurjchem-20 30 84     SPACE eurjchem-20 30 85 to to PART eurjchem-20 30 86     SPACE eurjchem-20 30 87 afford afford VERB eurjchem-20 30 88     SPACE eurjchem-20 30 89 pure pure ADJ eurjchem-20 30 90     SPACE eurjchem-20 30 91 4a­i 4a­i NUM eurjchem-20 30 92     SPACE eurjchem-20 30 93 which which PRON eurjchem-20 30 94     SPACE eurjchem-20 30 95 were be AUX eurjchem-20 30 96     SPACE eurjchem-20 30 97 characterized characterize VERB eurjchem-20 30 98     SPACE eurjchem-20 30 99 by by ADP eurjchem-20 30 100     SPACE eurjchem-20 30 101 ir ir PROPN eurjchem-20 30 102 , , PUNCT eurjchem-20 30 103     SPACE eurjchem-20 30 104 1h 1h NUM eurjchem-20 30 105 , , PUNCT eurjchem-20 30 106     SPACE eurjchem-20 30 107 13c 13c NOUN eurjchem-20 30 108 , , PUNCT eurjchem-20 30 109     SPACE eurjchem-20 30 110 31p 31p NUM eurjchem-20 30 111     SPACE eurjchem-20 30 112 nmr nmr NOUN eurjchem-20 30 113     SPACE eurjchem-20 30 114 and and CCONJ eurjchem-20 30 115     SPACE eurjchem-20 30 116 mass mass PROPN eurjchem-20 30 117     SPACE eurjchem-20 30 118 spectral spectral ADJ eurjchem-20 30 119     SPACE eurjchem-20 30 120 data datum NOUN eurjchem-20 30 121     SPACE eurjchem-20 30 122 analyses analysis NOUN eurjchem-20 30 123 . . PUNCT eurjchem-20 30 124           SPACE eurjchem-20 30 125 2.2.1 2.2.1 NUM eurjchem-20 30 126 . . PUNCT eurjchem-20 30 127     SPACE eurjchem-20 30 128 ( ( PUNCT eurjchem-20 30 129 r)­(5­(5­methyl­2,4­dioxo­3,4­dihydropyrimidin­ r)­(5­(5­methyl­2,4­dioxo­3,4­dihydropyrimidin­ NOUN eurjchem-20 30 130 1(2h)­yl)­2,5­dihydrofuran­2­yl)methyl­n 1(2h)­yl)­2,5­dihydrofuran­2­yl)methyl­n NUM eurjchem-20 30 131 , , PUNCT eurjchem-20 30 132 n­bis(2­chloro n­bis(2­chloro CCONJ eurjchem-20 30 133     SPACE eurjchem-20 30 134 ethyl)­p­(4­methylpiperazin­1­yl)phosphonamidate ethyl)­p­(4­methylpiperazin­1­yl)phosphonamidate NOUN eurjchem-20 30 135     SPACE eurjchem-20 30 136 ( ( PUNCT eurjchem-20 30 137 4a 4a NUM eurjchem-20 30 138 ) ) PUNCT eurjchem-20 30 139         SPACE eurjchem-20 30 140 yield yield NOUN eurjchem-20 30 141 : : PUNCT eurjchem-20 30 142     SPACE eurjchem-20 30 143 55 55 NUM eurjchem-20 30 144 % % NOUN eurjchem-20 30 145 . . PUNCT eurjchem-20 30 146     SPACE eurjchem-20 31 1 m.p m.p PROPN eurjchem-20 31 2 . . PROPN eurjchem-20 31 3 : : PUNCT eurjchem-20 31 4     SPACE eurjchem-20 31 5 155‐158 155‐158 NOUN eurjchem-20 31 6     SPACE eurjchem-20 31 7 oc oc PROPN eurjchem-20 31 8 . . PUNCT eurjchem-20 31 9     SPACE eurjchem-20 31 10 ir ir PROPN eurjchem-20 31 11     SPACE eurjchem-20 31 12 ( ( PUNCT eurjchem-20 31 13 kbr kbr PROPN eurjchem-20 31 14 , , PUNCT eurjchem-20 31 15     SPACE eurjchem-20 31 16 cm‐1 cm‐1 NOUN eurjchem-20 31 17 ): ): PUNCT eurjchem-20 31 18     SPACE eurjchem-20 31 19 3393 3393 NUM eurjchem-20 31 20     SPACE eurjchem-20 31 21 ν(‐nh ν(‐nh PROPN eurjchem-20 31 22 ) ) PUNCT eurjchem-20 31 23 , , PUNCT eurjchem-20 31 24     SPACE eurjchem-20 31 25 1683 1683 NUM eurjchem-20 31 26     SPACE eurjchem-20 31 27 ν(c ν(c PROPN eurjchem-20 31 28 = = SYM eurjchem-20 31 29 o o NOUN eurjchem-20 31 30 ) ) PUNCT eurjchem-20 31 31 , , PUNCT eurjchem-20 31 32     SPACE eurjchem-20 31 33 1226 1226 NUM eurjchem-20 31 34     SPACE eurjchem-20 31 35 ν(p ν(p NOUN eurjchem-20 31 36 = = SYM eurjchem-20 31 37 o o NOUN eurjchem-20 31 38 ) ) PUNCT eurjchem-20 31 39 . . PUNCT eurjchem-20 31 40     SPACE eurjchem-20 32 1 1h‐nmr 1h‐nmr NUM eurjchem-20 32 2     SPACE eurjchem-20 32 3 ( ( PUNCT eurjchem-20 32 4 500 500 NUM eurjchem-20 32 5     SPACE eurjchem-20 32 6 mhz mhz NOUN eurjchem-20 32 7 , , PUNCT eurjchem-20 32 8     SPACE eurjchem-20 32 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 32 10 , , PUNCT eurjchem-20 32 11     SPACE eurjchem-20 32 12   NUM eurjchem-20 32 13 ): ): PUNCT eurjchem-20 32 14     SPACE eurjchem-20 32 15 8.5(s 8.5(s NUM eurjchem-20 32 16 , , PUNCT eurjchem-20 32 17     SPACE eurjchem-20 32 18 1h 1h NUM eurjchem-20 32 19 , , PUNCT eurjchem-20 32 20     SPACE eurjchem-20 32 21 nh nh PROPN eurjchem-20 32 22 ) ) PUNCT eurjchem-20 32 23 , , PUNCT eurjchem-20 32 24     SPACE eurjchem-20 32 25 7.54 7.54 NUM eurjchem-20 32 26     SPACE eurjchem-20 32 27 ( ( PUNCT eurjchem-20 32 28 d d PROPN eurjchem-20 32 29 , , PUNCT eurjchem-20 32 30     SPACE eurjchem-20 32 31 1h 1h NUM eurjchem-20 32 32 , , PUNCT eurjchem-20 32 33     SPACE eurjchem-20 32 34 j=1.5 j=1.5 NOUN eurjchem-20 32 35     SPACE eurjchem-20 32 36 hz hz VERB eurjchem-20 32 37 , , PUNCT eurjchem-20 32 38     SPACE eurjchem-20 32 39 h‐6 h‐6 NOUN eurjchem-20 32 40 ) ) PUNCT eurjchem-20 32 41 , , PUNCT eurjchem-20 32 42     SPACE eurjchem-20 32 43 6.86‐6.88 6.86‐6.88 NUM eurjchem-20 32 44     SPACE eurjchem-20 32 45 ( ( PUNCT eurjchem-20 32 46 m m PROPN eurjchem-20 32 47 , , PUNCT eurjchem-20 32 48     SPACE eurjchem-20 32 49 1h 1h NUM eurjchem-20 32 50 , , PUNCT eurjchem-20 32 51     SPACE eurjchem-20 32 52 h‐ h‐ PROPN eurjchem-20 32 53 1 1 NUM eurjchem-20 32 54 ' ' NUM eurjchem-20 32 55 ) ) PUNCT eurjchem-20 32 56 , , PUNCT eurjchem-20 32 57     SPACE eurjchem-20 32 58 6.47‐6.49 6.47‐6.49 NUM eurjchem-20 32 59     SPACE eurjchem-20 32 60 ( ( PUNCT eurjchem-20 32 61 m m PROPN eurjchem-20 32 62 , , PUNCT eurjchem-20 32 63     SPACE eurjchem-20 32 64 1h 1h NUM eurjchem-20 32 65 , , PUNCT eurjchem-20 32 66     SPACE eurjchem-20 32 67 h‐2 h‐2 NOUN eurjchem-20 32 68 ' ' PUNCT eurjchem-20 32 69 ) ) PUNCT eurjchem-20 32 70 , , PUNCT eurjchem-20 32 71     SPACE eurjchem-20 32 72 5.95‐5.97 5.95‐5.97 NOUN eurjchem-20 32 73     SPACE eurjchem-20 32 74 ( ( PUNCT eurjchem-20 32 75 m m PROPN eurjchem-20 32 76 , , PUNCT eurjchem-20 32 77     SPACE eurjchem-20 32 78 1h 1h NUM eurjchem-20 32 79 , , PUNCT eurjchem-20 32 80     SPACE eurjchem-20 32 81 h‐3 h‐3 NOUN eurjchem-20 32 82 ' ' PUNCT eurjchem-20 32 83 ) ) PUNCT eurjchem-20 32 84 , , PUNCT eurjchem-20 32 85     SPACE eurjchem-20 32 86 4.13‐4.21 4.13‐4.21 NUM eurjchem-20 32 87     SPACE eurjchem-20 32 88 ( ( PUNCT eurjchem-20 32 89 m m PROPN eurjchem-20 32 90 , , PUNCT eurjchem-20 32 91     SPACE eurjchem-20 32 92 3h 3h NUM eurjchem-20 32 93 , , PUNCT eurjchem-20 32 94     SPACE eurjchem-20 32 95 h‐4 h‐4 NOUN eurjchem-20 32 96 ' ' PUNCT eurjchem-20 32 97 , , PUNCT eurjchem-20 32 98     SPACE eurjchem-20 32 99 2h‐5 2h‐5 NUM eurjchem-20 32 100 ' ' PUNCT eurjchem-20 32 101 ) ) PUNCT eurjchem-20 32 102 , , PUNCT eurjchem-20 32 103     SPACE eurjchem-20 32 104 3.95 3.95 NUM eurjchem-20 32 105     SPACE eurjchem-20 32 106 ( ( PUNCT eurjchem-20 32 107 t t PROPN eurjchem-20 32 108 , , PUNCT eurjchem-20 32 109     SPACE eurjchem-20 32 110 4h 4h NOUN eurjchem-20 32 111 , , PUNCT eurjchem-20 32 112     SPACE eurjchem-20 32 113 ch2‐n ch2‐n ADJ eurjchem-20 32 114 ) ) PUNCT eurjchem-20 32 115 , , PUNCT eurjchem-20 32 116     SPACE eurjchem-20 32 117 3.65 3.65 NUM eurjchem-20 32 118     SPACE eurjchem-20 32 119 ( ( PUNCT eurjchem-20 32 120 t t PROPN eurjchem-20 32 121 , , PUNCT eurjchem-20 32 122     SPACE eurjchem-20 32 123 4h 4h NOUN eurjchem-20 32 124 , , PUNCT eurjchem-20 32 125     SPACE eurjchem-20 32 126 ch2‐cl ch2‐cl NOUN eurjchem-20 32 127 ) ) PUNCT eurjchem-20 32 128 , , PUNCT eurjchem-20 32 129     SPACE eurjchem-20 32 130 2.74 2.74 NUM eurjchem-20 32 131     SPACE eurjchem-20 32 132 ( ( PUNCT eurjchem-20 32 133 t t PROPN eurjchem-20 32 134 , , PUNCT eurjchem-20 32 135     SPACE eurjchem-20 32 136 4h 4h NOUN eurjchem-20 32 137 , , PUNCT eurjchem-20 32 138     SPACE eurjchem-20 32 139 ch2n‐ ch2n‐ PROPN eurjchem-20 32 140 ) ) PUNCT eurjchem-20 32 141 , , PUNCT eurjchem-20 32 142     SPACE eurjchem-20 32 143 2.49 2.49 NUM eurjchem-20 32 144     SPACE eurjchem-20 32 145 ( ( PUNCT eurjchem-20 32 146 t t PROPN eurjchem-20 32 147 , , PUNCT eurjchem-20 32 148     SPACE eurjchem-20 32 149 4h 4h NOUN eurjchem-20 32 150 , , PUNCT eurjchem-20 32 151     SPACE eurjchem-20 32 152 ch2n ch2n PROPN eurjchem-20 32 153 ) ) PUNCT eurjchem-20 32 154 , , PUNCT eurjchem-20 32 155     SPACE eurjchem-20 32 156 2.32 2.32 NUM eurjchem-20 32 157     SPACE eurjchem-20 32 158 ( ( PUNCT eurjchem-20 32 159 s s PROPN eurjchem-20 32 160 , , PUNCT eurjchem-20 32 161     SPACE eurjchem-20 32 162 3h 3h NUM eurjchem-20 32 163 , , PUNCT eurjchem-20 32 164     SPACE eurjchem-20 32 165 n‐me n‐me NOUN eurjchem-20 32 166 ) ) PUNCT eurjchem-20 32 167 , , PUNCT eurjchem-20 32 168     SPACE eurjchem-20 32 169 1.87 1.87 NUM eurjchem-20 32 170     SPACE eurjchem-20 32 171 ( ( PUNCT eurjchem-20 32 172 s s PROPN eurjchem-20 32 173 , , PUNCT eurjchem-20 32 174     SPACE eurjchem-20 32 175 3h 3h NUM eurjchem-20 32 176 , , PUNCT eurjchem-20 32 177     SPACE eurjchem-20 32 178 ch3 ch3 PROPN eurjchem-20 32 179 ) ) PUNCT eurjchem-20 32 180 . . PUNCT eurjchem-20 32 181     SPACE eurjchem-20 33 1 13c‐nmr 13c‐nmr NOUN eurjchem-20 33 2     SPACE eurjchem-20 33 3 ( ( PUNCT eurjchem-20 33 4 125 125 NUM eurjchem-20 33 5     SPACE eurjchem-20 33 6 mhz mhz NOUN eurjchem-20 33 7 , , PUNCT eurjchem-20 33 8     SPACE eurjchem-20 33 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 33 10 ): ): PUNCT eurjchem-20 33 11     SPACE eurjchem-20 33 12 164.5 164.5 NUM eurjchem-20 33 13     SPACE eurjchem-20 33 14 ( ( PUNCT eurjchem-20 33 15 c‐4 c‐4 PROPN eurjchem-20 33 16 ) ) PUNCT eurjchem-20 33 17 , , PUNCT eurjchem-20 33 18     SPACE eurjchem-20 33 19 159.2 159.2 NUM eurjchem-20 33 20     SPACE eurjchem-20 33 21 ( ( PUNCT eurjchem-20 33 22 c‐2 c‐2 NOUN eurjchem-20 33 23 ) ) PUNCT eurjchem-20 33 24 , , PUNCT eurjchem-20 33 25     SPACE eurjchem-20 33 26 137 137 NUM eurjchem-20 33 27     SPACE eurjchem-20 33 28 ( ( PUNCT eurjchem-20 33 29 c‐6 c‐6 NOUN eurjchem-20 33 30 ) ) PUNCT eurjchem-20 33 31 , , PUNCT eurjchem-20 33 32     SPACE eurjchem-20 33 33 135.1(c‐3 135.1(c‐3 PROPN eurjchem-20 33 34 ' ' PUNCT eurjchem-20 33 35 ) ) PUNCT eurjchem-20 33 36 , , PUNCT eurjchem-20 33 37     SPACE eurjchem-20 33 38 125.1 125.1 NUM eurjchem-20 33 39     SPACE eurjchem-20 33 40 ( ( PUNCT eurjchem-20 33 41 c‐2 c‐2 NOUN eurjchem-20 33 42 ' ' PUNCT eurjchem-20 33 43 ) ) PUNCT eurjchem-20 33 44 , , PUNCT eurjchem-20 33 45     SPACE eurjchem-20 33 46 110.5 110.5 NUM eurjchem-20 33 47     SPACE eurjchem-20 33 48 ( ( PUNCT eurjchem-20 33 49 c‐5 c‐5 NOUN eurjchem-20 33 50 ) ) PUNCT eurjchem-20 33 51 , , PUNCT eurjchem-20 33 52     SPACE eurjchem-20 33 53 89.2 89.2 NUM eurjchem-20 33 54     SPACE eurjchem-20 33 55 ( ( PUNCT eurjchem-20 33 56 c‐ c‐ NOUN eurjchem-20 33 57 1 1 NUM eurjchem-20 33 58 ' ' NUM eurjchem-20 33 59 ) ) PUNCT eurjchem-20 33 60 , , PUNCT eurjchem-20 33 61     SPACE eurjchem-20 33 62 85.5 85.5 NUM eurjchem-20 33 63     SPACE eurjchem-20 33 64 ( ( PUNCT eurjchem-20 33 65 c‐4 c‐4 PROPN eurjchem-20 33 66 ' ' PUNCT eurjchem-20 33 67 ) ) PUNCT eurjchem-20 33 68 , , PUNCT eurjchem-20 33 69     SPACE eurjchem-20 33 70 68.2 68.2 NUM eurjchem-20 33 71     SPACE eurjchem-20 33 72 ( ( PUNCT eurjchem-20 33 73 c‐5 c‐5 NOUN eurjchem-20 33 74 ' ' PUNCT eurjchem-20 33 75 ) ) PUNCT eurjchem-20 33 76 , , PUNCT eurjchem-20 33 77     SPACE eurjchem-20 33 78 55.8 55.8 NUM eurjchem-20 33 79     SPACE eurjchem-20 33 80 ( ( PUNCT eurjchem-20 33 81 pipch2 pipch2 NOUN eurjchem-20 33 82 ) ) PUNCT eurjchem-20 33 83 , , PUNCT eurjchem-20 33 84     SPACE eurjchem-20 33 85 51.2 51.2 NUM eurjchem-20 33 86     SPACE eurjchem-20 33 87 ( ( PUNCT eurjchem-20 33 88 c‐2 c‐2 NOUN eurjchem-20 33 89 '' '' PUNCT eurjchem-20 33 90 ) ) PUNCT eurjchem-20 33 91 , , PUNCT eurjchem-20 33 92     SPACE eurjchem-20 33 93 47.8 47.8 NUM eurjchem-20 33 94     SPACE eurjchem-20 33 95 ( ( PUNCT eurjchem-20 33 96 pipch2 pipch2 NOUN eurjchem-20 33 97 ) ) PUNCT eurjchem-20 33 98 , , PUNCT eurjchem-20 33 99     SPACE eurjchem-20 33 100 45.9 45.9 NUM eurjchem-20 33 101     SPACE eurjchem-20 33 102 ( ( PUNCT eurjchem-20 33 103 n‐ch3 n‐ch3 PROPN eurjchem-20 33 104 ) ) PUNCT eurjchem-20 33 105 , , PUNCT eurjchem-20 33 106     SPACE eurjchem-20 33 107 41.6 41.6 NUM eurjchem-20 33 108     SPACE eurjchem-20 33 109 ( ( PUNCT eurjchem-20 33 110 c‐3 c‐3 NOUN eurjchem-20 33 111 '' '' PUNCT eurjchem-20 33 112 ) ) PUNCT eurjchem-20 33 113 , , PUNCT eurjchem-20 33 114     SPACE eurjchem-20 33 115 12.1 12.1 NUM eurjchem-20 33 116     SPACE eurjchem-20 33 117 ( ( PUNCT eurjchem-20 33 118 ‐ch3 ‐ch3 ADJ eurjchem-20 33 119 ) ) PUNCT eurjchem-20 33 120 . . PUNCT eurjchem-20 33 121     SPACE eurjchem-20 34 1 31p‐nmr 31p‐nmr NOUN eurjchem-20 34 2     SPACE eurjchem-20 34 3 ( ( PUNCT eurjchem-20 34 4 202 202 NUM eurjchem-20 34 5     SPACE eurjchem-20 34 6 mhz mhz NOUN eurjchem-20 34 7 , , PUNCT eurjchem-20 34 8     SPACE eurjchem-20 34 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 34 10 ): ): PUNCT eurjchem-20 34 11     SPACE eurjchem-20 34 12   NUM eurjchem-20 34 13     SPACE eurjchem-20 34 14 ‐1.94 ‐1.94 NUM eurjchem-20 34 15 , , PUNCT eurjchem-20 34 16     SPACE eurjchem-20 34 17 ‐1.24 ‐1.24 NOUN eurjchem-20 34 18 . . PUNCT eurjchem-20 34 19     SPACE eurjchem-20 35 1 gc‐ms gc‐ms NOUN eurjchem-20 35 2     SPACE eurjchem-20 35 3 ( ( PUNCT eurjchem-20 35 4 m m PROPN eurjchem-20 35 5 / / SYM eurjchem-20 35 6 z z NOUN eurjchem-20 35 7 , , PUNCT eurjchem-20 35 8     SPACE eurjchem-20 35 9 % % NOUN eurjchem-20 35 10 ): ): PUNCT eurjchem-20 35 11     SPACE eurjchem-20 35 12 ( ( PUNCT eurjchem-20 35 13 510.25 510.25 NUM eurjchem-20 35 14 , , PUNCT eurjchem-20 35 15     SPACE eurjchem-20 35 16 45 45 NUM eurjchem-20 35 17 % % NOUN eurjchem-20 35 18 ) ) PUNCT eurjchem-20 35 19     SPACE eurjchem-20 36 1 [ [ X eurjchem-20 36 2 mh]+ mh]+ X eurjchem-20 36 3 . . PUNCT eurjchem-20 36 4           SPACE eurjchem-20 36 5 2.2.2 2.2.2 NUM eurjchem-20 36 6 . . PUNCT eurjchem-20 36 7     SPACE eurjchem-20 36 8 ( ( PUNCT eurjchem-20 36 9 r)­(5­(5­methyl­2,4­dioxo­3,4­dihydropyrimidin­ r)­(5­(5­methyl­2,4­dioxo­3,4­dihydropyrimidin­ NOUN eurjchem-20 36 10 1(2h)­yl)­2,5­dihydrofuran­2­yl)methyl­n 1(2h)­yl)­2,5­dihydrofuran­2­yl)methyl­n NUM eurjchem-20 36 11 , , PUNCT eurjchem-20 36 12 n­bis(2­chloro n­bis(2­chloro CCONJ eurjchem-20 36 13     SPACE eurjchem-20 36 14 ethyl)­p­(piperazin­1­yl)phosphonamidate ethyl)­p­(piperazin­1­yl)phosphonamidate NOUN eurjchem-20 36 15     SPACE eurjchem-20 36 16 ( ( PUNCT eurjchem-20 36 17 4b 4b X eurjchem-20 36 18 ) ) PUNCT eurjchem-20 36 19         SPACE eurjchem-20 36 20 yield yield NOUN eurjchem-20 36 21 : : PUNCT eurjchem-20 36 22     SPACE eurjchem-20 36 23 62 62 NUM eurjchem-20 36 24 % % NOUN eurjchem-20 36 25 . . PUNCT eurjchem-20 36 26     SPACE eurjchem-20 37 1 m.p m.p PROPN eurjchem-20 37 2 . . PROPN eurjchem-20 37 3 : : PUNCT eurjchem-20 37 4     SPACE eurjchem-20 37 5 161‐163 161‐163 NUM eurjchem-20 37 6     SPACE eurjchem-20 37 7 oc oc NOUN eurjchem-20 37 8 , , PUNCT eurjchem-20 37 9     SPACE eurjchem-20 37 10 anal anal ADJ eurjchem-20 37 11 . . PUNCT eurjchem-20 37 12     SPACE eurjchem-20 37 13 calcd calcd NOUN eurjchem-20 37 14 . . PUNCT eurjchem-20 37 15     SPACE eurjchem-20 37 16 for for ADP eurjchem-20 37 17     SPACE eurjchem-20 37 18 c18h28cl2n5o5p c18h28cl2n5o5p NOUN eurjchem-20 37 19 : : PUNCT eurjchem-20 37 20     SPACE eurjchem-20 37 21 c c X eurjchem-20 37 22 , , PUNCT eurjchem-20 37 23     SPACE eurjchem-20 37 24 43.56 43.56 NUM eurjchem-20 37 25 ; ; PUNCT eurjchem-20 37 26     SPACE eurjchem-20 37 27 h h NOUN eurjchem-20 37 28 , , PUNCT eurjchem-20 37 29     SPACE eurjchem-20 37 30 5.69 5.69 NUM eurjchem-20 37 31 ; ; PUNCT eurjchem-20 37 32     SPACE eurjchem-20 37 33 n n CCONJ eurjchem-20 37 34 , , PUNCT eurjchem-20 37 35     SPACE eurjchem-20 37 36 14.11 14.11 NUM eurjchem-20 37 37 ; ; PUNCT eurjchem-20 37 38     SPACE eurjchem-20 37 39 found find VERB eurjchem-20 37 40     SPACE eurjchem-20 37 41 c c NOUN eurjchem-20 37 42 , , PUNCT eurjchem-20 37 43     SPACE eurjchem-20 37 44 43.59 43.59 NUM eurjchem-20 37 45 ; ; PUNCT eurjchem-20 37 46     SPACE eurjchem-20 37 47 h h NOUN eurjchem-20 37 48 , , PUNCT eurjchem-20 37 49     SPACE eurjchem-20 37 50 5.73 5.73 NUM eurjchem-20 37 51 ; ; PUNCT eurjchem-20 37 52     SPACE eurjchem-20 37 53 n n CCONJ eurjchem-20 37 54 , , PUNCT eurjchem-20 37 55     SPACE eurjchem-20 37 56 14.05 14.05 NUM eurjchem-20 37 57 . . PUNCT eurjchem-20 37 58     SPACE eurjchem-20 38 1 ir ir VERB eurjchem-20 38 2     SPACE eurjchem-20 38 3 ( ( PUNCT eurjchem-20 38 4 kbr kbr PROPN eurjchem-20 38 5 , , PUNCT eurjchem-20 38 6     SPACE eurjchem-20 38 7 cm‐1 cm‐1 NOUN eurjchem-20 38 8 ): ): PUNCT eurjchem-20 38 9     SPACE eurjchem-20 38 10 3386 3386 NUM eurjchem-20 38 11     SPACE eurjchem-20 38 12 ν(‐nh ν(‐nh PROPN eurjchem-20 38 13 ) ) PUNCT eurjchem-20 38 14 , , PUNCT eurjchem-20 38 15     SPACE eurjchem-20 38 16 1685 1685 NUM eurjchem-20 38 17     SPACE eurjchem-20 38 18 ν(c ν(c PROPN eurjchem-20 38 19 = = SYM eurjchem-20 38 20 o o NOUN eurjchem-20 38 21 ) ) PUNCT eurjchem-20 38 22 , , PUNCT eurjchem-20 38 23     SPACE eurjchem-20 38 24 1230 1230 NUM eurjchem-20 38 25     SPACE eurjchem-20 38 26 ν(p ν(p PROPN eurjchem-20 38 27 = = SYM eurjchem-20 38 28 o o NOUN eurjchem-20 38 29 ) ) PUNCT eurjchem-20 38 30 . . PUNCT eurjchem-20 38 31     SPACE eurjchem-20 39 1 1h‐nmr 1h‐nmr NUM eurjchem-20 39 2     SPACE eurjchem-20 39 3 ( ( PUNCT eurjchem-20 39 4 500 500 NUM eurjchem-20 39 5     SPACE eurjchem-20 39 6 mhz mhz NOUN eurjchem-20 39 7 , , PUNCT eurjchem-20 39 8     SPACE eurjchem-20 39 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 39 10 , , PUNCT eurjchem-20 39 11     SPACE eurjchem-20 39 12   NUM eurjchem-20 39 13 ): ): PUNCT eurjchem-20 39 14         SPACE eurjchem-20 39 15 8.9 8.9 NUM eurjchem-20 39 16     SPACE eurjchem-20 39 17 ( ( PUNCT eurjchem-20 39 18 s s PROPN eurjchem-20 39 19 , , PUNCT eurjchem-20 39 20     SPACE eurjchem-20 39 21 1h 1h NUM eurjchem-20 39 22 , , PUNCT eurjchem-20 39 23     SPACE eurjchem-20 39 24 nh nh PROPN eurjchem-20 39 25 ) ) PUNCT eurjchem-20 39 26 , , PUNCT eurjchem-20 39 27     SPACE eurjchem-20 39 28 7.56 7.56 NUM eurjchem-20 39 29     SPACE eurjchem-20 39 30 ( ( PUNCT eurjchem-20 39 31 d d PROPN eurjchem-20 39 32 , , PUNCT eurjchem-20 39 33     SPACE eurjchem-20 39 34 1h 1h NUM eurjchem-20 39 35 , , PUNCT eurjchem-20 39 36     SPACE eurjchem-20 39 37 j=1.5 j=1.5 NOUN eurjchem-20 39 38     SPACE eurjchem-20 39 39 hz hz VERB eurjchem-20 39 40 , , PUNCT eurjchem-20 39 41     SPACE eurjchem-20 39 42 h‐6 h‐6 NOUN eurjchem-20 39 43 ) ) PUNCT eurjchem-20 39 44 , , PUNCT eurjchem-20 39 45     SPACE eurjchem-20 40 1 6.88‐6.9 6.88‐6.9 NUM eurjchem-20 40 2     SPACE eurjchem-20 40 3 ( ( PUNCT eurjchem-20 40 4 m m PROPN eurjchem-20 40 5 , , PUNCT eurjchem-20 40 6     SPACE eurjchem-20 40 7 1h 1h NUM eurjchem-20 40 8 , , PUNCT eurjchem-20 40 9     SPACE eurjchem-20 40 10 h‐1 h‐1 PROPN eurjchem-20 40 11 ' ' PUNCT eurjchem-20 40 12 ) ) PUNCT eurjchem-20 40 13 , , PUNCT eurjchem-20 40 14     SPACE eurjchem-20 40 15 6.47‐6.49 6.47‐6.49 NUM eurjchem-20 40 16     SPACE eurjchem-20 40 17 ( ( PUNCT eurjchem-20 40 18 m m PROPN eurjchem-20 40 19 , , PUNCT eurjchem-20 40 20     SPACE eurjchem-20 40 21 1h 1h NUM eurjchem-20 40 22 , , PUNCT eurjchem-20 40 23     SPACE eurjchem-20 40 24 h‐2 h‐2 NOUN eurjchem-20 40 25 ' ' PUNCT eurjchem-20 40 26 ) ) PUNCT eurjchem-20 40 27 , , PUNCT eurjchem-20 40 28     SPACE eurjchem-20 40 29 5.97‐5.99 5.97‐5.99 NUM eurjchem-20 40 30     SPACE eurjchem-20 40 31 ( ( PUNCT eurjchem-20 40 32 m m PROPN eurjchem-20 40 33 , , PUNCT eurjchem-20 40 34     SPACE eurjchem-20 40 35 1h 1h NUM eurjchem-20 40 36 , , PUNCT eurjchem-20 40 37     SPACE eurjchem-20 40 38 h‐3 h‐3 NOUN eurjchem-20 40 39 ' ' PUNCT eurjchem-20 40 40 ) ) PUNCT eurjchem-20 40 41 , , PUNCT eurjchem-20 40 42     SPACE eurjchem-20 40 43 4.15‐4.23 4.15‐4.23 NUM eurjchem-20 40 44     SPACE eurjchem-20 40 45 ( ( PUNCT eurjchem-20 40 46 m m PROPN eurjchem-20 40 47 , , PUNCT eurjchem-20 40 48     SPACE eurjchem-20 40 49 3h 3h NUM eurjchem-20 40 50 , , PUNCT eurjchem-20 40 51     SPACE eurjchem-20 40 52 h‐4 h‐4 NOUN eurjchem-20 40 53 ' ' PUNCT eurjchem-20 40 54 , , PUNCT eurjchem-20 40 55     SPACE eurjchem-20 40 56 2h‐5 2h‐5 NUM eurjchem-20 40 57 ' ' PUNCT eurjchem-20 40 58 ) ) PUNCT eurjchem-20 40 59 , , PUNCT eurjchem-20 40 60     SPACE eurjchem-20 40 61 4.01 4.01 NUM eurjchem-20 40 62     SPACE eurjchem-20 40 63 ( ( PUNCT eurjchem-20 40 64 t t PROPN eurjchem-20 40 65 , , PUNCT eurjchem-20 40 66     SPACE eurjchem-20 40 67 4h 4h NOUN eurjchem-20 40 68 , , PUNCT eurjchem-20 40 69     SPACE eurjchem-20 40 70 ch2‐n ch2‐n ADJ eurjchem-20 40 71 ) ) PUNCT eurjchem-20 40 72 , , PUNCT eurjchem-20 40 73     SPACE eurjchem-20 40 74 3.69 3.69 NUM eurjchem-20 40 75     SPACE eurjchem-20 40 76 ( ( PUNCT eurjchem-20 40 77 t t PROPN eurjchem-20 40 78 , , PUNCT eurjchem-20 40 79     SPACE eurjchem-20 40 80 4h 4h NOUN eurjchem-20 40 81 , , PUNCT eurjchem-20 40 82     SPACE eurjchem-20 40 83 ch2‐cl ch2‐cl NOUN eurjchem-20 40 84 ) ) PUNCT eurjchem-20 40 85 , , PUNCT eurjchem-20 40 86     SPACE eurjchem-20 40 87 2.78 2.78 NUM eurjchem-20 40 88     SPACE eurjchem-20 40 89 ( ( PUNCT eurjchem-20 40 90 t t PROPN eurjchem-20 40 91 , , PUNCT eurjchem-20 40 92     SPACE eurjchem-20 40 93 4h 4h NOUN eurjchem-20 40 94 , , PUNCT eurjchem-20 40 95     SPACE eurjchem-20 40 96 ch2n‐ ch2n‐ PROPN eurjchem-20 40 97 ) ) PUNCT eurjchem-20 40 98 , , PUNCT eurjchem-20 40 99     SPACE eurjchem-20 40 100 2.54 2.54 NUM eurjchem-20 40 101     SPACE eurjchem-20 40 102 rao rao PROPN eurjchem-20 40 103     SPACE eurjchem-20 40 104 et et PROPN eurjchem-20 40 105     SPACE eurjchem-20 40 106 al al PROPN eurjchem-20 40 107 . . PROPN eurjchem-20 40 108     SPACE eurjchem-20 40 109 / / SYM eurjchem-20 40 110     SPACE eurjchem-20 40 111 european european ADJ eurjchem-20 40 112     SPACE eurjchem-20 40 113 journal journal NOUN eurjchem-20 40 114     SPACE eurjchem-20 40 115 of of ADP eurjchem-20 40 116     SPACE eurjchem-20 40 117 chemistry chemistry NOUN eurjchem-20 40 118     SPACE eurjchem-20 40 119 1 1 NUM eurjchem-20 40 120     SPACE eurjchem-20 40 121 ( ( PUNCT eurjchem-20 40 122 4 4 NUM eurjchem-20 40 123 ) ) PUNCT eurjchem-20 40 124     SPACE eurjchem-20 40 125 ( ( PUNCT eurjchem-20 40 126 2010 2010 NUM eurjchem-20 40 127 ) ) PUNCT eurjchem-20 40 128     SPACE eurjchem-20 40 129 297­301 297­301 NOUN eurjchem-20 40 130     SPACE eurjchem-20 40 131 299 299 NUM eurjchem-20 40 132     SPACE eurjchem-20 40 133 ( ( PUNCT eurjchem-20 40 134 t t PROPN eurjchem-20 40 135 , , PUNCT eurjchem-20 40 136     SPACE eurjchem-20 40 137 4h 4h NOUN eurjchem-20 40 138 , , PUNCT eurjchem-20 40 139     SPACE eurjchem-20 40 140 ch2nh ch2nh NOUN eurjchem-20 40 141 ) ) PUNCT eurjchem-20 40 142 , , PUNCT eurjchem-20 40 143     SPACE eurjchem-20 40 144 2.19 2.19 NUM eurjchem-20 40 145     SPACE eurjchem-20 40 146 ( ( PUNCT eurjchem-20 40 147 s s PROPN eurjchem-20 40 148 , , PUNCT eurjchem-20 40 149     SPACE eurjchem-20 40 150 1h 1h NUM eurjchem-20 40 151 , , PUNCT eurjchem-20 40 152     SPACE eurjchem-20 40 153 nh nh PROPN eurjchem-20 40 154 ) ) PUNCT eurjchem-20 40 155 , , PUNCT eurjchem-20 40 156     SPACE eurjchem-20 40 157 1.87 1.87 NUM eurjchem-20 40 158     SPACE eurjchem-20 40 159 ( ( PUNCT eurjchem-20 40 160 s s PROPN eurjchem-20 40 161 , , PUNCT eurjchem-20 40 162     SPACE eurjchem-20 40 163 3h 3h NUM eurjchem-20 40 164 , , PUNCT eurjchem-20 40 165     SPACE eurjchem-20 40 166 ch3 ch3 PROPN eurjchem-20 40 167 ) ) PUNCT eurjchem-20 40 168 . . PUNCT eurjchem-20 40 169     SPACE eurjchem-20 41 1 31p‐nmr 31p‐nmr NOUN eurjchem-20 41 2     SPACE eurjchem-20 41 3 ( ( PUNCT eurjchem-20 41 4 202 202 NUM eurjchem-20 41 5     SPACE eurjchem-20 41 6 mhz mhz NOUN eurjchem-20 41 7 , , PUNCT eurjchem-20 41 8     SPACE eurjchem-20 41 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 41 10 , , PUNCT eurjchem-20 41 11     SPACE eurjchem-20 41 12   NUM eurjchem-20 41 13 ) ) PUNCT eurjchem-20 41 14     SPACE eurjchem-20 41 15 ‐1.03 ‐1.03 NUM eurjchem-20 41 16 . . PUNCT eurjchem-20 41 17         SPACE eurjchem-20 42 1 2.2.3 2.2.3 NUM eurjchem-20 42 2 . . PUNCT eurjchem-20 42 3     SPACE eurjchem-20 42 4 ( ( PUNCT eurjchem-20 42 5 r)­(5­(5­methyl­2,4­dioxo­3,4­dihydropyrimidin­ r)­(5­(5­methyl­2,4­dioxo­3,4­dihydropyrimidin­ NOUN eurjchem-20 42 6 1(2h)­yl)­2,5­dihydrofuran­2­yl)methyl­n 1(2h)­yl)­2,5­dihydrofuran­2­yl)methyl­n NUM eurjchem-20 42 7 , , PUNCT eurjchem-20 42 8 n­bis(2­chloro n­bis(2­chloro CCONJ eurjchem-20 42 9     SPACE eurjchem-20 42 10 ethyl)­p­(piperidin ethyl)­p­(piperidin VERB eurjchem-20 42 11     SPACE eurjchem-20 42 12 ­1­yl ­1­yl NOUN eurjchem-20 42 13 ) ) PUNCT eurjchem-20 42 14     SPACE eurjchem-20 42 15 phosphonamidate phosphonamidate NOUN eurjchem-20 42 16     SPACE eurjchem-20 42 17 ( ( PUNCT eurjchem-20 42 18 4c 4c NOUN eurjchem-20 42 19 ) ) PUNCT eurjchem-20 42 20         SPACE eurjchem-20 42 21 yield yield NOUN eurjchem-20 42 22 : : PUNCT eurjchem-20 42 23     SPACE eurjchem-20 42 24 61 61 NUM eurjchem-20 42 25 % % NOUN eurjchem-20 42 26 . . PUNCT eurjchem-20 42 27     SPACE eurjchem-20 43 1 m.p m.p PROPN eurjchem-20 43 2 . . PROPN eurjchem-20 43 3 : : PUNCT eurjchem-20 43 4     SPACE eurjchem-20 43 5 174‐176 174‐176 PROPN eurjchem-20 43 6     SPACE eurjchem-20 43 7 oc oc PROPN eurjchem-20 43 8 , , PUNCT eurjchem-20 43 9     SPACE eurjchem-20 43 10 anal anal ADJ eurjchem-20 43 11 . . PUNCT eurjchem-20 43 12     SPACE eurjchem-20 43 13 calcd calcd NOUN eurjchem-20 43 14 . . PUNCT eurjchem-20 43 15     SPACE eurjchem-20 43 16 for for ADP eurjchem-20 43 17     SPACE eurjchem-20 43 18 c19h29cl2n4o5p c19h29cl2n4o5p NOUN eurjchem-20 43 19 : : PUNCT eurjchem-20 43 20     SPACE eurjchem-20 43 21 c c X eurjchem-20 43 22 , , PUNCT eurjchem-20 43 23     SPACE eurjchem-20 43 24 46.07 46.07 NUM eurjchem-20 43 25 ; ; PUNCT eurjchem-20 43 26     SPACE eurjchem-20 43 27 h h NOUN eurjchem-20 43 28 , , PUNCT eurjchem-20 43 29     SPACE eurjchem-20 43 30 5.90 5.90 NUM eurjchem-20 43 31 ; ; PUNCT eurjchem-20 43 32     SPACE eurjchem-20 43 33 n n CCONJ eurjchem-20 43 34 , , PUNCT eurjchem-20 43 35     SPACE eurjchem-20 43 36 11.31 11.31 NUM eurjchem-20 43 37 ; ; PUNCT eurjchem-20 43 38     SPACE eurjchem-20 43 39 found find VERB eurjchem-20 43 40     SPACE eurjchem-20 43 41 c c NOUN eurjchem-20 43 42 , , PUNCT eurjchem-20 43 43     SPACE eurjchem-20 43 44 46.12 46.12 NUM eurjchem-20 43 45 . . PUNCT eurjchem-20 43 46 ; ; PUNCT eurjchem-20 43 47     SPACE eurjchem-20 43 48 h h NOUN eurjchem-20 43 49 , , PUNCT eurjchem-20 43 50     SPACE eurjchem-20 43 51 5.95 5.95 NUM eurjchem-20 43 52 ; ; PUNCT eurjchem-20 43 53     SPACE eurjchem-20 43 54 n n CCONJ eurjchem-20 43 55 , , PUNCT eurjchem-20 43 56     SPACE eurjchem-20 43 57 11.25 11.25 NUM eurjchem-20 43 58 . . PUNCT eurjchem-20 43 59     SPACE eurjchem-20 44 1 ir ir VERB eurjchem-20 44 2     SPACE eurjchem-20 44 3 ( ( PUNCT eurjchem-20 44 4 kbr kbr PROPN eurjchem-20 44 5 , , PUNCT eurjchem-20 44 6     SPACE eurjchem-20 44 7 cm‐1 cm‐1 NOUN eurjchem-20 44 8 ): ): PUNCT eurjchem-20 44 9     SPACE eurjchem-20 44 10 3378 3378 NUM eurjchem-20 44 11     SPACE eurjchem-20 44 12 ν(‐nh ν(‐nh PROPN eurjchem-20 44 13 ) ) PUNCT eurjchem-20 44 14 , , PUNCT eurjchem-20 44 15     SPACE eurjchem-20 44 16 1686 1686 NUM eurjchem-20 44 17     SPACE eurjchem-20 44 18 ν(c ν(c PROPN eurjchem-20 44 19 = = SYM eurjchem-20 44 20 o o NOUN eurjchem-20 44 21 ) ) PUNCT eurjchem-20 44 22 , , PUNCT eurjchem-20 44 23     SPACE eurjchem-20 44 24 1234 1234 NUM eurjchem-20 44 25     SPACE eurjchem-20 44 26 ν(p ν(p PROPN eurjchem-20 44 27 = = SYM eurjchem-20 44 28 o o NOUN eurjchem-20 44 29 ) ) PUNCT eurjchem-20 44 30 . . PUNCT eurjchem-20 44 31     SPACE eurjchem-20 45 1 1h‐nmr 1h‐nmr NUM eurjchem-20 45 2     SPACE eurjchem-20 45 3 ( ( PUNCT eurjchem-20 45 4 500 500 NUM eurjchem-20 45 5     SPACE eurjchem-20 45 6 mhz mhz NOUN eurjchem-20 45 7 , , PUNCT eurjchem-20 45 8     SPACE eurjchem-20 45 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 45 10 , , PUNCT eurjchem-20 45 11     SPACE eurjchem-20 45 12   NUM eurjchem-20 45 13 ): ): PUNCT eurjchem-20 45 14     SPACE eurjchem-20 45 15 8.8 8.8 NUM eurjchem-20 45 16     SPACE eurjchem-20 45 17 ( ( PUNCT eurjchem-20 45 18 s s PROPN eurjchem-20 45 19 , , PUNCT eurjchem-20 45 20     SPACE eurjchem-20 45 21 1h 1h NUM eurjchem-20 45 22 , , PUNCT eurjchem-20 45 23     SPACE eurjchem-20 45 24 nh nh PROPN eurjchem-20 45 25 ) ) PUNCT eurjchem-20 45 26 , , PUNCT eurjchem-20 45 27     SPACE eurjchem-20 45 28 7.5 7.5 NUM eurjchem-20 45 29     SPACE eurjchem-20 45 30 ( ( PUNCT eurjchem-20 45 31 d d PROPN eurjchem-20 45 32 , , PUNCT eurjchem-20 45 33     SPACE eurjchem-20 45 34 1h 1h NUM eurjchem-20 45 35 , , PUNCT eurjchem-20 45 36     SPACE eurjchem-20 45 37 j=1.5 j=1.5 NOUN eurjchem-20 45 38     SPACE eurjchem-20 45 39 hz hz VERB eurjchem-20 45 40 , , PUNCT eurjchem-20 45 41     SPACE eurjchem-20 45 42 h‐6 h‐6 NOUN eurjchem-20 45 43 ) ) PUNCT eurjchem-20 45 44 , , PUNCT eurjchem-20 45 45     SPACE eurjchem-20 45 46 6.84‐6.88 6.84‐6.88 NUM eurjchem-20 45 47     SPACE eurjchem-20 45 48 ( ( PUNCT eurjchem-20 45 49 m m PROPN eurjchem-20 45 50 , , PUNCT eurjchem-20 45 51     SPACE eurjchem-20 45 52 1h 1h NUM eurjchem-20 45 53 , , PUNCT eurjchem-20 45 54     SPACE eurjchem-20 45 55 h‐1 h‐1 PROPN eurjchem-20 45 56 ' ' PUNCT eurjchem-20 45 57 ) ) PUNCT eurjchem-20 45 58 , , PUNCT eurjchem-20 45 59     SPACE eurjchem-20 45 60 6.46‐6.48 6.46‐6.48 NOUN eurjchem-20 45 61     SPACE eurjchem-20 45 62 ( ( PUNCT eurjchem-20 45 63 m m PROPN eurjchem-20 45 64 , , PUNCT eurjchem-20 45 65     SPACE eurjchem-20 45 66 1h 1h NUM eurjchem-20 45 67 , , PUNCT eurjchem-20 45 68     SPACE eurjchem-20 45 69 h‐ h‐ PROPN eurjchem-20 45 70 2 2 NUM eurjchem-20 45 71 ' ' NUM eurjchem-20 45 72 ) ) PUNCT eurjchem-20 45 73 , , PUNCT eurjchem-20 45 74     SPACE eurjchem-20 45 75 5.93‐5.95 5.93‐5.95 NOUN eurjchem-20 45 76     SPACE eurjchem-20 45 77 ( ( PUNCT eurjchem-20 45 78 m m PROPN eurjchem-20 45 79 , , PUNCT eurjchem-20 45 80     SPACE eurjchem-20 45 81 1h 1h NUM eurjchem-20 45 82 , , PUNCT eurjchem-20 45 83     SPACE eurjchem-20 45 84 h‐3 h‐3 NOUN eurjchem-20 45 85 ' ' PUNCT eurjchem-20 45 86 ) ) PUNCT eurjchem-20 45 87 , , PUNCT eurjchem-20 45 88     SPACE eurjchem-20 45 89 4.15‐4.28 4.15‐4.28 NOUN eurjchem-20 45 90     SPACE eurjchem-20 45 91 ( ( PUNCT eurjchem-20 45 92 m m PROPN eurjchem-20 45 93 , , PUNCT eurjchem-20 45 94     SPACE eurjchem-20 45 95 3h 3h NUM eurjchem-20 45 96 , , PUNCT eurjchem-20 45 97     SPACE eurjchem-20 45 98 h‐4 h‐4 NOUN eurjchem-20 45 99 ' ' PUNCT eurjchem-20 45 100 , , PUNCT eurjchem-20 45 101     SPACE eurjchem-20 45 102 2h‐5 2h‐5 NOUN eurjchem-20 45 103 ' ' PUNCT eurjchem-20 45 104 ) ) PUNCT eurjchem-20 45 105 , , PUNCT eurjchem-20 45 106     SPACE eurjchem-20 45 107 3.94 3.94 NUM eurjchem-20 45 108     SPACE eurjchem-20 45 109 ( ( PUNCT eurjchem-20 45 110 t t PROPN eurjchem-20 45 111 , , PUNCT eurjchem-20 45 112     SPACE eurjchem-20 45 113 4h 4h NOUN eurjchem-20 45 114 , , PUNCT eurjchem-20 45 115     SPACE eurjchem-20 45 116 ch2n ch2n PROPN eurjchem-20 45 117 ) ) PUNCT eurjchem-20 45 118 , , PUNCT eurjchem-20 45 119     SPACE eurjchem-20 45 120 3.63 3.63 NUM eurjchem-20 45 121     SPACE eurjchem-20 45 122 ( ( PUNCT eurjchem-20 45 123 t t PROPN eurjchem-20 45 124 , , PUNCT eurjchem-20 45 125     SPACE eurjchem-20 45 126 4h 4h NOUN eurjchem-20 45 127 , , PUNCT eurjchem-20 45 128     SPACE eurjchem-20 45 129 ‐ch2cl ‐ch2cl NOUN eurjchem-20 45 130 ) ) PUNCT eurjchem-20 45 131 , , PUNCT eurjchem-20 45 132     SPACE eurjchem-20 45 133 2.75(t 2.75(t PROPN eurjchem-20 45 134 , , PUNCT eurjchem-20 45 135     SPACE eurjchem-20 45 136 4h 4h NUM eurjchem-20 45 137 , , PUNCT eurjchem-20 45 138     SPACE eurjchem-20 45 139 ch2n‐ ch2n‐ PROPN eurjchem-20 45 140 ) ) PUNCT eurjchem-20 45 141 , , PUNCT eurjchem-20 45 142     SPACE eurjchem-20 45 143 1.87 1.87 NUM eurjchem-20 45 144     SPACE eurjchem-20 45 145 ( ( PUNCT eurjchem-20 45 146 s s PROPN eurjchem-20 45 147 , , PUNCT eurjchem-20 45 148     SPACE eurjchem-20 45 149 3h 3h NUM eurjchem-20 45 150 , , PUNCT eurjchem-20 45 151     SPACE eurjchem-20 45 152 ch3),1.46‐1.56(m ch3),1.46‐1.56(m PROPN eurjchem-20 45 153 , , PUNCT eurjchem-20 45 154     SPACE eurjchem-20 45 155 6h 6h NOUN eurjchem-20 45 156 , , PUNCT eurjchem-20 45 157     SPACE eurjchem-20 45 158 ( ( PUNCT eurjchem-20 45 159 ch2)3 ch2)3 PROPN eurjchem-20 45 160 ) ) PUNCT eurjchem-20 45 161 . . PUNCT eurjchem-20 45 162     SPACE eurjchem-20 46 1 31p‐nmr 31p‐nmr NOUN eurjchem-20 46 2     SPACE eurjchem-20 46 3 ( ( PUNCT eurjchem-20 46 4 202 202 NUM eurjchem-20 46 5     SPACE eurjchem-20 46 6 mhz mhz NOUN eurjchem-20 46 7 , , PUNCT eurjchem-20 46 8     SPACE eurjchem-20 46 9 dmso‐ dmso‐ PROPN eurjchem-20 46 10 d6 d6 NOUN eurjchem-20 46 11 , , PUNCT eurjchem-20 46 12     SPACE eurjchem-20 46 13   NUM eurjchem-20 46 14 ): ): PUNCT eurjchem-20 46 15     SPACE eurjchem-20 46 16 2.85 2.85 NUM eurjchem-20 46 17 . . PUNCT eurjchem-20 46 18             SPACE eurjchem-20 46 19 2.2.4 2.2.4 NUM eurjchem-20 46 20 . . PUNCT eurjchem-20 46 21     SPACE eurjchem-20 46 22 ( ( PUNCT eurjchem-20 46 23 r)­(5­(5­methyl­2,4­dioxo­3,4­dihydropyrimidin­ r)­(5­(5­methyl­2,4­dioxo­3,4­dihydropyrimidin­ NOUN eurjchem-20 46 24 1(2h)­yl)­2,5­dihydrofuran­2­yl)methyl­n 1(2h)­yl)­2,5­dihydrofuran­2­yl)methyl­n NUM eurjchem-20 46 25 , , PUNCT eurjchem-20 46 26 n­bis(2­chloro n­bis(2­chloro CCONJ eurjchem-20 46 27     SPACE eurjchem-20 46 28 ethyl)­p­morpholinophosphonamidate ethyl)­p­morpholinophosphonamidate NOUN eurjchem-20 46 29     SPACE eurjchem-20 46 30 ( ( PUNCT eurjchem-20 46 31 4d 4d NUM eurjchem-20 46 32 ) ) PUNCT eurjchem-20 46 33         SPACE eurjchem-20 46 34 yield yield NOUN eurjchem-20 46 35 : : PUNCT eurjchem-20 46 36     SPACE eurjchem-20 46 37 55 55 NUM eurjchem-20 46 38 % % NOUN eurjchem-20 46 39 . . PUNCT eurjchem-20 46 40     SPACE eurjchem-20 47 1 m.p m.p PROPN eurjchem-20 47 2 . . PROPN eurjchem-20 47 3 : : PUNCT eurjchem-20 47 4     SPACE eurjchem-20 47 5 167‐169 167‐169 NUM eurjchem-20 47 6     SPACE eurjchem-20 47 7 0c 0c NOUN eurjchem-20 47 8 , , PUNCT eurjchem-20 47 9     SPACE eurjchem-20 47 10 ir ir PROPN eurjchem-20 47 11     SPACE eurjchem-20 47 12 ( ( PUNCT eurjchem-20 47 13 kbr kbr PROPN eurjchem-20 47 14 , , PUNCT eurjchem-20 47 15     SPACE eurjchem-20 47 16 cm‐1 cm‐1 NOUN eurjchem-20 47 17 ): ): PUNCT eurjchem-20 47 18     SPACE eurjchem-20 47 19 3394 3394 NUM eurjchem-20 47 20     SPACE eurjchem-20 47 21 ν(‐nh ν(‐nh PROPN eurjchem-20 47 22 ) ) PUNCT eurjchem-20 47 23 , , PUNCT eurjchem-20 47 24     SPACE eurjchem-20 47 25 1685 1685 NUM eurjchem-20 47 26     SPACE eurjchem-20 47 27 ν(c ν(c PROPN eurjchem-20 47 28 = = SYM eurjchem-20 47 29 o o NOUN eurjchem-20 47 30 ) ) PUNCT eurjchem-20 47 31 , , PUNCT eurjchem-20 47 32     SPACE eurjchem-20 47 33 1225 1225 NUM eurjchem-20 47 34     SPACE eurjchem-20 47 35 ν(p ν(p NOUN eurjchem-20 47 36 = = SYM eurjchem-20 47 37 o o NOUN eurjchem-20 47 38 ) ) PUNCT eurjchem-20 47 39 . . PUNCT eurjchem-20 47 40     SPACE eurjchem-20 48 1 1h‐nmr 1h‐nmr NUM eurjchem-20 48 2     SPACE eurjchem-20 48 3 ( ( PUNCT eurjchem-20 48 4 500 500 NUM eurjchem-20 48 5     SPACE eurjchem-20 48 6 mhz mhz NOUN eurjchem-20 48 7 , , PUNCT eurjchem-20 48 8     SPACE eurjchem-20 48 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 48 10 , , PUNCT eurjchem-20 48 11     SPACE eurjchem-20 48 12   NUM eurjchem-20 48 13 ): ): PUNCT eurjchem-20 48 14     SPACE eurjchem-20 48 15 8.6 8.6 NUM eurjchem-20 48 16     SPACE eurjchem-20 48 17 ( ( PUNCT eurjchem-20 48 18 s s PROPN eurjchem-20 48 19 , , PUNCT eurjchem-20 48 20     SPACE eurjchem-20 48 21 1h 1h NUM eurjchem-20 48 22 , , PUNCT eurjchem-20 48 23     SPACE eurjchem-20 48 24 nh nh PROPN eurjchem-20 48 25 ) ) PUNCT eurjchem-20 48 26 , , PUNCT eurjchem-20 48 27     SPACE eurjchem-20 48 28 7.7 7.7 NUM eurjchem-20 48 29     SPACE eurjchem-20 48 30 ( ( PUNCT eurjchem-20 48 31 d d NOUN eurjchem-20 48 32 , , PUNCT eurjchem-20 48 33     SPACE eurjchem-20 48 34 1h 1h NUM eurjchem-20 48 35 , , PUNCT eurjchem-20 48 36     SPACE eurjchem-20 48 37 j=1.5 j=1.5 NOUN eurjchem-20 48 38     SPACE eurjchem-20 48 39 hz hz VERB eurjchem-20 48 40 , , PUNCT eurjchem-20 48 41     SPACE eurjchem-20 48 42 h‐6 h‐6 NOUN eurjchem-20 48 43 ) ) PUNCT eurjchem-20 48 44 , , PUNCT eurjchem-20 48 45     SPACE eurjchem-20 48 46 6.95 6.95 NUM eurjchem-20 48 47     SPACE eurjchem-20 48 48 ‐6.97 ‐6.97 NOUN eurjchem-20 48 49     SPACE eurjchem-20 48 50 ( ( PUNCT eurjchem-20 48 51 m m PROPN eurjchem-20 48 52 , , PUNCT eurjchem-20 48 53     SPACE eurjchem-20 48 54 1h 1h NUM eurjchem-20 48 55 , , PUNCT eurjchem-20 48 56     SPACE eurjchem-20 48 57 h‐1 h‐1 PROPN eurjchem-20 48 58 ' ' PUNCT eurjchem-20 48 59 ) ) PUNCT eurjchem-20 48 60 , , PUNCT eurjchem-20 48 61     SPACE eurjchem-20 48 62 6.45‐6.47 6.45‐6.47 NUM eurjchem-20 48 63     SPACE eurjchem-20 48 64 ( ( PUNCT eurjchem-20 48 65 m m PROPN eurjchem-20 48 66 , , PUNCT eurjchem-20 48 67     SPACE eurjchem-20 48 68 1h 1h NUM eurjchem-20 48 69 , , PUNCT eurjchem-20 48 70     SPACE eurjchem-20 48 71 h‐2 h‐2 NOUN eurjchem-20 48 72 ' ' PUNCT eurjchem-20 48 73 ) ) PUNCT eurjchem-20 48 74 , , PUNCT eurjchem-20 48 75     SPACE eurjchem-20 48 76 5.9‐5.92 5.9‐5.92 NUM eurjchem-20 48 77     SPACE eurjchem-20 48 78 ( ( PUNCT eurjchem-20 48 79 m m PROPN eurjchem-20 48 80 , , PUNCT eurjchem-20 48 81     SPACE eurjchem-20 48 82 1h 1h NUM eurjchem-20 48 83 , , PUNCT eurjchem-20 48 84     SPACE eurjchem-20 48 85 h‐3 h‐3 NOUN eurjchem-20 48 86 ' ' PUNCT eurjchem-20 48 87 ) ) PUNCT eurjchem-20 48 88 , , PUNCT eurjchem-20 48 89     SPACE eurjchem-20 48 90 4.15‐4.23 4.15‐4.23 NUM eurjchem-20 48 91     SPACE eurjchem-20 48 92 ( ( PUNCT eurjchem-20 48 93 m m PROPN eurjchem-20 48 94 , , PUNCT eurjchem-20 48 95     SPACE eurjchem-20 48 96 3h 3h NUM eurjchem-20 48 97 , , PUNCT eurjchem-20 48 98     SPACE eurjchem-20 48 99 h‐4 h‐4 NOUN eurjchem-20 48 100 ' ' PUNCT eurjchem-20 48 101 , , PUNCT eurjchem-20 48 102     SPACE eurjchem-20 48 103 2h‐5 2h‐5 NOUN eurjchem-20 48 104 ' ' PUNCT eurjchem-20 48 105 ) ) PUNCT eurjchem-20 48 106 , , PUNCT eurjchem-20 48 107     SPACE eurjchem-20 48 108 3.66 3.66 NUM eurjchem-20 48 109     SPACE eurjchem-20 48 110 ( ( PUNCT eurjchem-20 48 111 t t PROPN eurjchem-20 48 112 , , PUNCT eurjchem-20 48 113     SPACE eurjchem-20 48 114 4h 4h NOUN eurjchem-20 48 115 , , PUNCT eurjchem-20 48 116     SPACE eurjchem-20 48 117 ch2‐o ch2‐o NOUN eurjchem-20 48 118 ) ) PUNCT eurjchem-20 48 119 , , PUNCT eurjchem-20 48 120     SPACE eurjchem-20 48 121 3.6 3.6 NUM eurjchem-20 48 122     SPACE eurjchem-20 48 123 ( ( PUNCT eurjchem-20 48 124 t t PROPN eurjchem-20 48 125 , , PUNCT eurjchem-20 48 126     SPACE eurjchem-20 48 127 4h 4h NOUN eurjchem-20 48 128 , , PUNCT eurjchem-20 48 129     SPACE eurjchem-20 48 130 ch2n ch2n PROPN eurjchem-20 48 131 ) ) PUNCT eurjchem-20 48 132 , , PUNCT eurjchem-20 48 133     SPACE eurjchem-20 48 134 3.06 3.06 NUM eurjchem-20 48 135     SPACE eurjchem-20 48 136 ( ( PUNCT eurjchem-20 48 137 t t PROPN eurjchem-20 48 138 , , PUNCT eurjchem-20 48 139     SPACE eurjchem-20 48 140 4h 4h NOUN eurjchem-20 48 141 , , PUNCT eurjchem-20 48 142     SPACE eurjchem-20 48 143 ch2‐cl ch2‐cl NOUN eurjchem-20 48 144 ) ) PUNCT eurjchem-20 48 145 , , PUNCT eurjchem-20 48 146     SPACE eurjchem-20 48 147 2.64 2.64 NUM eurjchem-20 48 148     SPACE eurjchem-20 48 149 ( ( PUNCT eurjchem-20 48 150 t t PROPN eurjchem-20 48 151 , , PUNCT eurjchem-20 48 152     SPACE eurjchem-20 48 153 4h 4h NOUN eurjchem-20 48 154 , , PUNCT eurjchem-20 48 155     SPACE eurjchem-20 48 156 ch2n‐ ch2n‐ PROPN eurjchem-20 48 157 ) ) PUNCT eurjchem-20 48 158 , , PUNCT eurjchem-20 48 159     SPACE eurjchem-20 48 160 1.0 1.0 NUM eurjchem-20 48 161     SPACE eurjchem-20 48 162 ( ( PUNCT eurjchem-20 48 163 s s PROPN eurjchem-20 48 164 , , PUNCT eurjchem-20 48 165     SPACE eurjchem-20 48 166 3h 3h NUM eurjchem-20 48 167 , , PUNCT eurjchem-20 48 168     SPACE eurjchem-20 48 169 ch3 ch3 PROPN eurjchem-20 48 170 ) ) PUNCT eurjchem-20 48 171 . . PUNCT eurjchem-20 48 172     SPACE eurjchem-20 49 1 13c‐nmr 13c‐nmr NOUN eurjchem-20 49 2     SPACE eurjchem-20 49 3 ( ( PUNCT eurjchem-20 49 4 125 125 NUM eurjchem-20 49 5     SPACE eurjchem-20 49 6 mhz mhz NOUN eurjchem-20 49 7 , , PUNCT eurjchem-20 49 8     SPACE eurjchem-20 49 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 49 10 ): ): PUNCT eurjchem-20 49 11     SPACE eurjchem-20 49 12 163.9 163.9 NUM eurjchem-20 49 13     SPACE eurjchem-20 49 14 ( ( PUNCT eurjchem-20 49 15 c‐4 c‐4 PROPN eurjchem-20 49 16 ) ) PUNCT eurjchem-20 49 17 , , PUNCT eurjchem-20 49 18     SPACE eurjchem-20 49 19 158.4 158.4 NUM eurjchem-20 49 20     SPACE eurjchem-20 49 21 ( ( PUNCT eurjchem-20 49 22 c‐2 c‐2 NOUN eurjchem-20 49 23 ) ) PUNCT eurjchem-20 49 24 , , PUNCT eurjchem-20 49 25     SPACE eurjchem-20 49 26 136.5 136.5 NUM eurjchem-20 49 27     SPACE eurjchem-20 49 28 ( ( PUNCT eurjchem-20 49 29 c‐6 c‐6 NOUN eurjchem-20 49 30 ) ) PUNCT eurjchem-20 49 31 , , PUNCT eurjchem-20 49 32     SPACE eurjchem-20 49 33 134.5(c‐ 134.5(c‐ NUM eurjchem-20 49 34 3 3 NUM eurjchem-20 49 35 ' ' NUM eurjchem-20 49 36 ) ) PUNCT eurjchem-20 49 37 , , PUNCT eurjchem-20 49 38     SPACE eurjchem-20 49 39 125.8 125.8 NUM eurjchem-20 49 40     SPACE eurjchem-20 49 41 ( ( PUNCT eurjchem-20 49 42 c‐2 c‐2 NOUN eurjchem-20 49 43 ' ' PUNCT eurjchem-20 49 44 ) ) PUNCT eurjchem-20 49 45 , , PUNCT eurjchem-20 49 46     SPACE eurjchem-20 49 47 111.2 111.2 NUM eurjchem-20 49 48     SPACE eurjchem-20 49 49 ( ( PUNCT eurjchem-20 49 50 c‐5 c‐5 NOUN eurjchem-20 49 51 ) ) PUNCT eurjchem-20 49 52 , , PUNCT eurjchem-20 49 53     SPACE eurjchem-20 49 54 91.2 91.2 NUM eurjchem-20 49 55     SPACE eurjchem-20 49 56 ( ( PUNCT eurjchem-20 49 57 c‐1 c‐1 NOUN eurjchem-20 49 58 ' ' PUNCT eurjchem-20 49 59 ) ) PUNCT eurjchem-20 49 60 , , PUNCT eurjchem-20 49 61     SPACE eurjchem-20 49 62 86.5 86.5 NUM eurjchem-20 49 63     SPACE eurjchem-20 49 64 ( ( PUNCT eurjchem-20 49 65 c‐4 c‐4 PROPN eurjchem-20 49 66 ' ' PUNCT eurjchem-20 49 67 ) ) PUNCT eurjchem-20 49 68 , , PUNCT eurjchem-20 49 69     SPACE eurjchem-20 49 70 69.2 69.2 NUM eurjchem-20 49 71     SPACE eurjchem-20 49 72 ( ( PUNCT eurjchem-20 49 73 c‐5 c‐5 NOUN eurjchem-20 49 74 ' ' PUNCT eurjchem-20 49 75 ) ) PUNCT eurjchem-20 49 76 , , PUNCT eurjchem-20 49 77     SPACE eurjchem-20 49 78 62.8 62.8 NUM eurjchem-20 49 79     SPACE eurjchem-20 49 80 ( ( PUNCT eurjchem-20 49 81 morch2 morch2 PROPN eurjchem-20 49 82 ) ) PUNCT eurjchem-20 49 83 , , PUNCT eurjchem-20 49 84     SPACE eurjchem-20 49 85 52.5 52.5 NUM eurjchem-20 49 86     SPACE eurjchem-20 49 87 ( ( PUNCT eurjchem-20 49 88 c‐2 c‐2 NOUN eurjchem-20 49 89 '' '' PUNCT eurjchem-20 49 90 ) ) PUNCT eurjchem-20 49 91 , , PUNCT eurjchem-20 49 92     SPACE eurjchem-20 49 93 45.8 45.8 NUM eurjchem-20 49 94     SPACE eurjchem-20 49 95 ( ( PUNCT eurjchem-20 49 96 morch2 morch2 PROPN eurjchem-20 49 97 ) ) PUNCT eurjchem-20 49 98 , , PUNCT eurjchem-20 49 99     SPACE eurjchem-20 49 100 42.6 42.6 NUM eurjchem-20 49 101     SPACE eurjchem-20 49 102 ( ( PUNCT eurjchem-20 49 103 c‐3 c‐3 NOUN eurjchem-20 49 104 '' '' PUNCT eurjchem-20 49 105 ) ) PUNCT eurjchem-20 49 106 , , PUNCT eurjchem-20 49 107     SPACE eurjchem-20 49 108 12.1 12.1 NUM eurjchem-20 49 109     SPACE eurjchem-20 49 110 ( ( PUNCT eurjchem-20 49 111 ‐ ‐ PROPN eurjchem-20 49 112 ch3 ch3 PROPN eurjchem-20 49 113 ) ) PUNCT eurjchem-20 49 114 . . PUNCT eurjchem-20 49 115     SPACE eurjchem-20 50 1 31p‐nmr 31p‐nmr NOUN eurjchem-20 50 2     SPACE eurjchem-20 50 3 ( ( PUNCT eurjchem-20 50 4 202 202 NUM eurjchem-20 50 5     SPACE eurjchem-20 50 6 mhz mhz NOUN eurjchem-20 50 7 , , PUNCT eurjchem-20 50 8     SPACE eurjchem-20 50 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 50 10 , , PUNCT eurjchem-20 50 11     SPACE eurjchem-20 50 12   NUM eurjchem-20 50 13 ): ): PUNCT eurjchem-20 50 14     SPACE eurjchem-20 50 15 ‐2.15 ‐2.15 ADJ eurjchem-20 50 16 , , PUNCT eurjchem-20 50 17     SPACE eurjchem-20 50 18 ‐1.51 ‐1.51 PROPN eurjchem-20 50 19 . . PUNCT eurjchem-20 50 20     SPACE eurjchem-20 51 1 gcms gcms PROPN eurjchem-20 51 2     SPACE eurjchem-20 51 3 ( ( PUNCT eurjchem-20 51 4 m m PROPN eurjchem-20 51 5 / / SYM eurjchem-20 51 6 z z NOUN eurjchem-20 51 7 ; ; PUNCT eurjchem-20 51 8     SPACE eurjchem-20 51 9 % % NOUN eurjchem-20 51 10 ): ): PUNCT eurjchem-20 51 11     SPACE eurjchem-20 51 12 ( ( PUNCT eurjchem-20 51 13 497.25 497.25 NUM eurjchem-20 51 14 , , PUNCT eurjchem-20 51 15     SPACE eurjchem-20 51 16 30 30 NUM eurjchem-20 51 17 % % NOUN eurjchem-20 51 18 ) ) PUNCT eurjchem-20 51 19     SPACE eurjchem-20 52 1 [ [ X eurjchem-20 52 2 mh]+ mh]+ X eurjchem-20 52 3 . . PUNCT eurjchem-20 52 4           SPACE eurjchem-20 52 5 2.2.5 2.2.5 NUM eurjchem-20 52 6 . . PUNCT eurjchem-20 52 7     SPACE eurjchem-20 52 8 ethyl2­((s)­((5­(5­methyl­2,4­dioxo­3,4­dihydro ethyl2­((s)­((5­(5­methyl­2,4­dioxo­3,4­dihydro NOUN eurjchem-20 52 9     SPACE eurjchem-20 52 10 pyrimidin­1(2h)­yl)­2,5­dihydrofuran­2­yl)methoxy pyrimidin­1(2h)­yl)­2,5­dihydrofuran­2­yl)methoxy NOUN eurjchem-20 52 11 ) ) PUNCT eurjchem-20 52 12     SPACE eurjchem-20 53 1 ( ( PUNCT eurjchem-20 53 2 4­ 4­ PROPN eurjchem-20 53 3 nitrophenoxy nitrophenoxy ADJ eurjchem-20 53 4 ) ) PUNCT eurjchem-20 53 5     SPACE eurjchem-20 53 6 phosphorylamino)­2­phenylacetate phosphorylamino)­2­phenylacetate NOUN eurjchem-20 53 7     SPACE eurjchem-20 53 8 ( ( PUNCT eurjchem-20 53 9 4e 4e NOUN eurjchem-20 53 10 ) ) PUNCT eurjchem-20 53 11         SPACE eurjchem-20 53 12 yield yield NOUN eurjchem-20 53 13 : : PUNCT eurjchem-20 53 14     SPACE eurjchem-20 53 15 59 59 NUM eurjchem-20 53 16 % % NOUN eurjchem-20 53 17 . . PUNCT eurjchem-20 53 18     SPACE eurjchem-20 54 1 m.p m.p PROPN eurjchem-20 54 2 . . PROPN eurjchem-20 54 3 : : PUNCT eurjchem-20 54 4     SPACE eurjchem-20 54 5 149‐152 149‐152 NUM eurjchem-20 54 6     SPACE eurjchem-20 54 7 oc oc PROPN eurjchem-20 54 8 , , PUNCT eurjchem-20 54 9     SPACE eurjchem-20 54 10 ir ir NOUN eurjchem-20 54 11     SPACE eurjchem-20 54 12 ( ( PUNCT eurjchem-20 54 13 kbr kbr PROPN eurjchem-20 54 14 , , PUNCT eurjchem-20 54 15     SPACE eurjchem-20 54 16 cm‐1 cm‐1 NOUN eurjchem-20 54 17 ): ): PUNCT eurjchem-20 54 18     SPACE eurjchem-20 54 19 3389 3389 NUM eurjchem-20 54 20     SPACE eurjchem-20 54 21 ν(‐nh ν(‐nh PROPN eurjchem-20 54 22 ) ) PUNCT eurjchem-20 54 23 , , PUNCT eurjchem-20 54 24     SPACE eurjchem-20 54 25 1681 1681 NUM eurjchem-20 54 26 , , PUNCT eurjchem-20 54 27     SPACE eurjchem-20 54 28 1729 1729 NUM eurjchem-20 54 29     SPACE eurjchem-20 54 30 ν(c ν(c PROPN eurjchem-20 54 31 = = NOUN eurjchem-20 54 32 o o NOUN eurjchem-20 54 33 ) ) PUNCT eurjchem-20 54 34 , , PUNCT eurjchem-20 54 35     SPACE eurjchem-20 54 36 1236 1236 NUM eurjchem-20 54 37     SPACE eurjchem-20 54 38 ν(p ν(p NOUN eurjchem-20 54 39 = = SYM eurjchem-20 54 40 o o NOUN eurjchem-20 54 41 ) ) PUNCT eurjchem-20 54 42 . . PUNCT eurjchem-20 54 43     SPACE eurjchem-20 55 1 1h‐nmr 1h‐nmr NUM eurjchem-20 55 2     SPACE eurjchem-20 55 3 ( ( PUNCT eurjchem-20 55 4 500 500 NUM eurjchem-20 55 5     SPACE eurjchem-20 55 6 mhz mhz NOUN eurjchem-20 55 7 , , PUNCT eurjchem-20 55 8     SPACE eurjchem-20 55 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 55 10 , , PUNCT eurjchem-20 55 11     SPACE eurjchem-20 55 12   NUM eurjchem-20 55 13 ): ): PUNCT eurjchem-20 55 14     SPACE eurjchem-20 55 15 11.2 11.2 NUM eurjchem-20 55 16     SPACE eurjchem-20 55 17 ( ( PUNCT eurjchem-20 55 18 s s PROPN eurjchem-20 55 19 , , PUNCT eurjchem-20 55 20     SPACE eurjchem-20 55 21 1h 1h NUM eurjchem-20 55 22 , , PUNCT eurjchem-20 55 23     SPACE eurjchem-20 55 24 nh nh PROPN eurjchem-20 55 25 ) ) PUNCT eurjchem-20 55 26 , , PUNCT eurjchem-20 55 27     SPACE eurjchem-20 55 28 8.16 8.16 NUM eurjchem-20 55 29     SPACE eurjchem-20 55 30 ( ( PUNCT eurjchem-20 55 31 d d PROPN eurjchem-20 55 32 , , PUNCT eurjchem-20 55 33     SPACE eurjchem-20 55 34 2h 2h NUM eurjchem-20 55 35 , , PUNCT eurjchem-20 55 36     SPACE eurjchem-20 55 37 j=9 j=9 NOUN eurjchem-20 55 38     SPACE eurjchem-20 55 39 hz hz VERB eurjchem-20 55 40 , , PUNCT eurjchem-20 55 41     SPACE eurjchem-20 55 42 ar‐h ar‐h NOUN eurjchem-20 55 43 ) ) PUNCT eurjchem-20 55 44 , , PUNCT eurjchem-20 55 45     SPACE eurjchem-20 55 46 8.1 8.1 NUM eurjchem-20 55 47     SPACE eurjchem-20 55 48 ( ( PUNCT eurjchem-20 55 49 d d NOUN eurjchem-20 55 50 , , PUNCT eurjchem-20 55 51     SPACE eurjchem-20 55 52 2h 2h NUM eurjchem-20 55 53 , , PUNCT eurjchem-20 55 54     SPACE eurjchem-20 55 55 j=9.5 j=9.5 NOUN eurjchem-20 55 56     SPACE eurjchem-20 55 57 hz hz VERB eurjchem-20 55 58 , , PUNCT eurjchem-20 55 59     SPACE eurjchem-20 55 60 ar‐h ar‐h NOUN eurjchem-20 55 61 ) ) PUNCT eurjchem-20 55 62 , , PUNCT eurjchem-20 55 63     SPACE eurjchem-20 55 64 7.57 7.57 NUM eurjchem-20 55 65     SPACE eurjchem-20 55 66 ( ( PUNCT eurjchem-20 55 67 d d PROPN eurjchem-20 55 68 , , PUNCT eurjchem-20 55 69     SPACE eurjchem-20 55 70 1h 1h NUM eurjchem-20 55 71 , , PUNCT eurjchem-20 55 72     SPACE eurjchem-20 55 73 j=1 j=1 NOUN eurjchem-20 55 74     SPACE eurjchem-20 55 75 hz hz VERB eurjchem-20 55 76 , , PUNCT eurjchem-20 55 77     SPACE eurjchem-20 55 78 h‐6 h‐6 NOUN eurjchem-20 55 79 ) ) PUNCT eurjchem-20 55 80 , , PUNCT eurjchem-20 55 81     SPACE eurjchem-20 56 1 7.23‐7.4 7.23‐7.4 NUM eurjchem-20 56 2     SPACE eurjchem-20 56 3 ( ( PUNCT eurjchem-20 56 4 m m PROPN eurjchem-20 56 5 , , PUNCT eurjchem-20 56 6     SPACE eurjchem-20 56 7 5h 5h NUM eurjchem-20 56 8 , , PUNCT eurjchem-20 56 9     SPACE eurjchem-20 56 10 ar‐h ar‐h NOUN eurjchem-20 56 11 ) ) PUNCT eurjchem-20 56 12 , , PUNCT eurjchem-20 56 13     SPACE eurjchem-20 56 14 6.8‐ 6.8‐ NUM eurjchem-20 56 15 6.81 6.81 NUM eurjchem-20 56 16     SPACE eurjchem-20 56 17 ( ( PUNCT eurjchem-20 56 18 m m PROPN eurjchem-20 56 19 , , PUNCT eurjchem-20 56 20     SPACE eurjchem-20 56 21 1h 1h NUM eurjchem-20 56 22 , , PUNCT eurjchem-20 56 23     SPACE eurjchem-20 56 24 h‐1 h‐1 PROPN eurjchem-20 56 25 ' ' PUNCT eurjchem-20 56 26 ) ) PUNCT eurjchem-20 56 27 , , PUNCT eurjchem-20 56 28     SPACE eurjchem-20 56 29 6.31‐6.33 6.31‐6.33 NOUN eurjchem-20 56 30     SPACE eurjchem-20 56 31 ( ( PUNCT eurjchem-20 56 32 m m PROPN eurjchem-20 56 33 , , PUNCT eurjchem-20 56 34     SPACE eurjchem-20 56 35 1h 1h NUM eurjchem-20 56 36 , , PUNCT eurjchem-20 56 37     SPACE eurjchem-20 56 38 h‐2 h‐2 NOUN eurjchem-20 56 39 ' ' PUNCT eurjchem-20 56 40 ) ) PUNCT eurjchem-20 56 41 , , PUNCT eurjchem-20 56 42     SPACE eurjchem-20 56 43 5.89‐5.90 5.89‐5.90 NUM eurjchem-20 56 44     SPACE eurjchem-20 56 45 ( ( PUNCT eurjchem-20 56 46 m m PROPN eurjchem-20 56 47 , , PUNCT eurjchem-20 56 48     SPACE eurjchem-20 56 49 1h 1h NUM eurjchem-20 56 50 , , PUNCT eurjchem-20 56 51     SPACE eurjchem-20 56 52 h‐ h‐ PROPN eurjchem-20 56 53 3 3 NUM eurjchem-20 56 54 ' ' NUM eurjchem-20 56 55 ) ) PUNCT eurjchem-20 56 56 , , PUNCT eurjchem-20 56 57     SPACE eurjchem-20 56 58 6.54 6.54 NUM eurjchem-20 56 59     SPACE eurjchem-20 56 60 ( ( PUNCT eurjchem-20 56 61 brs br VERB eurjchem-20 56 62 , , PUNCT eurjchem-20 56 63     SPACE eurjchem-20 56 64 1h 1h NUM eurjchem-20 56 65 , , PUNCT eurjchem-20 56 66     SPACE eurjchem-20 56 67 gly‐nh gly‐nh PROPN eurjchem-20 56 68 ) ) PUNCT eurjchem-20 56 69 , , PUNCT eurjchem-20 56 70     SPACE eurjchem-20 56 71 3.57‐3.63 3.57‐3.63 NUM eurjchem-20 56 72     SPACE eurjchem-20 56 73 ( ( PUNCT eurjchem-20 56 74 m m PROPN eurjchem-20 56 75 , , PUNCT eurjchem-20 56 76     SPACE eurjchem-20 56 77 4h 4h NOUN eurjchem-20 56 78 , , PUNCT eurjchem-20 56 79     SPACE eurjchem-20 56 80 2h‐5 2h‐5 NUM eurjchem-20 56 81 ' ' PUNCT eurjchem-20 56 82 , , PUNCT eurjchem-20 56 83     SPACE eurjchem-20 56 84 h‐4 h‐4 NOUN eurjchem-20 56 85 ' ' PUNCT eurjchem-20 56 86 , , PUNCT eurjchem-20 56 87     SPACE eurjchem-20 56 88 gly‐ gly‐ NOUN eurjchem-20 56 89 nh‐ch nh‐ch NUM eurjchem-20 56 90 ) ) PUNCT eurjchem-20 56 91 , , PUNCT eurjchem-20 56 92     SPACE eurjchem-20 56 93 3.04 3.04 NUM eurjchem-20 56 94     SPACE eurjchem-20 56 95 ( ( PUNCT eurjchem-20 56 96 q q NOUN eurjchem-20 56 97 , , PUNCT eurjchem-20 56 98     SPACE eurjchem-20 56 99 2h 2h NUM eurjchem-20 56 100 , , PUNCT eurjchem-20 56 101     SPACE eurjchem-20 56 102 ‐och2 ‐och2 NOUN eurjchem-20 56 103 ) ) PUNCT eurjchem-20 56 104 , , PUNCT eurjchem-20 56 105     SPACE eurjchem-20 56 106 1.73 1.73 NUM eurjchem-20 56 107     SPACE eurjchem-20 56 108 ( ( PUNCT eurjchem-20 56 109 s s PROPN eurjchem-20 56 110 , , PUNCT eurjchem-20 56 111     SPACE eurjchem-20 56 112 3h 3h NUM eurjchem-20 56 113 , , PUNCT eurjchem-20 56 114     SPACE eurjchem-20 56 115 ch3 ch3 PROPN eurjchem-20 56 116 ) ) PUNCT eurjchem-20 56 117 , , PUNCT eurjchem-20 56 118     SPACE eurjchem-20 56 119 1.2 1.2 NUM eurjchem-20 56 120     SPACE eurjchem-20 56 121 ( ( PUNCT eurjchem-20 56 122 t t PROPN eurjchem-20 56 123 , , PUNCT eurjchem-20 56 124     SPACE eurjchem-20 56 125 3h 3h NUM eurjchem-20 56 126 , , PUNCT eurjchem-20 56 127     SPACE eurjchem-20 56 128 o‐ch2‐ o‐ch2‐ PROPN eurjchem-20 56 129 ch3 ch3 PROPN eurjchem-20 56 130 ) ) PUNCT eurjchem-20 56 131 . . PUNCT eurjchem-20 56 132     SPACE eurjchem-20 57 1 13c‐nmr 13c‐nmr NOUN eurjchem-20 57 2     SPACE eurjchem-20 57 3 ( ( PUNCT eurjchem-20 57 4 125 125 NUM eurjchem-20 57 5     SPACE eurjchem-20 57 6 mhz mhz NOUN eurjchem-20 57 7 , , PUNCT eurjchem-20 57 8     SPACE eurjchem-20 57 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 57 10 ): ): PUNCT eurjchem-20 57 11     SPACE eurjchem-20 57 12 171 171 NUM eurjchem-20 57 13     SPACE eurjchem-20 57 14 ( ( PUNCT eurjchem-20 57 15 gly gly ADV eurjchem-20 57 16     SPACE eurjchem-20 57 17 co co NOUN eurjchem-20 57 18 ) ) PUNCT eurjchem-20 57 19 , , PUNCT eurjchem-20 57 20     SPACE eurjchem-20 57 21 164.3 164.3 NUM eurjchem-20 57 22     SPACE eurjchem-20 57 23 ( ( PUNCT eurjchem-20 57 24 c‐4 c‐4 PROPN eurjchem-20 57 25 ) ) PUNCT eurjchem-20 57 26 , , PUNCT eurjchem-20 57 27     SPACE eurjchem-20 57 28 161.2 161.2 NUM eurjchem-20 57 29     SPACE eurjchem-20 57 30 ( ( PUNCT eurjchem-20 57 31 c‐1 c‐1 NOUN eurjchem-20 57 32 '' '' PUNCT eurjchem-20 57 33 ) ) PUNCT eurjchem-20 57 34 , , PUNCT eurjchem-20 57 35     SPACE eurjchem-20 57 36 151.2 151.2 NUM eurjchem-20 57 37     SPACE eurjchem-20 57 38 ( ( PUNCT eurjchem-20 57 39 c‐2 c‐2 NOUN eurjchem-20 57 40 ) ) PUNCT eurjchem-20 57 41 , , PUNCT eurjchem-20 57 42     SPACE eurjchem-20 57 43 142 142 NUM eurjchem-20 57 44     SPACE eurjchem-20 57 45 ( ( PUNCT eurjchem-20 57 46 c‐4 c‐4 PROPN eurjchem-20 57 47 '' '' PUNCT eurjchem-20 57 48 ) ) PUNCT eurjchem-20 57 49 , , PUNCT eurjchem-20 57 50     SPACE eurjchem-20 57 51 137.1 137.1 NUM eurjchem-20 57 52     SPACE eurjchem-20 57 53 ( ( PUNCT eurjchem-20 57 54 c‐6 c‐6 NOUN eurjchem-20 57 55 ) ) PUNCT eurjchem-20 57 56 , , PUNCT eurjchem-20 57 57     SPACE eurjchem-20 57 58 134.6 134.6 NUM eurjchem-20 57 59     SPACE eurjchem-20 57 60 ( ( PUNCT eurjchem-20 57 61 glyarc1 glyarc1 ADJ eurjchem-20 57 62 ) ) PUNCT eurjchem-20 57 63 , , PUNCT eurjchem-20 57 64     SPACE eurjchem-20 57 65 129.2 129.2 NUM eurjchem-20 57 66     SPACE eurjchem-20 57 67 ( ( PUNCT eurjchem-20 57 68 c‐3 c‐3 NOUN eurjchem-20 57 69 ' ' PUNCT eurjchem-20 57 70 ) ) PUNCT eurjchem-20 57 71 , , PUNCT eurjchem-20 57 72     SPACE eurjchem-20 57 73 128.7 128.7 NUM eurjchem-20 57 74     SPACE eurjchem-20 57 75 ( ( PUNCT eurjchem-20 57 76 glyarc‐2 glyarc‐2 NOUN eurjchem-20 57 77     SPACE eurjchem-20 57 78 & & CCONJ eurjchem-20 57 79     SPACE eurjchem-20 57 80 c‐6 c‐6 NOUN eurjchem-20 57 81 ) ) PUNCT eurjchem-20 57 82 , , PUNCT eurjchem-20 57 83     SPACE eurjchem-20 57 84 128.1 128.1 NUM eurjchem-20 57 85     SPACE eurjchem-20 57 86 ( ( PUNCT eurjchem-20 57 87 glyarc‐ glyarc‐ NOUN eurjchem-20 57 88 3 3 NOUN eurjchem-20 57 89     SPACE eurjchem-20 57 90 & & CCONJ eurjchem-20 57 91     SPACE eurjchem-20 57 92 c‐5 c‐5 NOUN eurjchem-20 57 93 ) ) PUNCT eurjchem-20 57 94 , , PUNCT eurjchem-20 57 95     SPACE eurjchem-20 57 96 127.5 127.5 NUM eurjchem-20 57 97     SPACE eurjchem-20 57 98 ( ( PUNCT eurjchem-20 57 99 glyarc‐4 glyarc‐4 PROPN eurjchem-20 57 100 ) ) PUNCT eurjchem-20 57 101 , , PUNCT eurjchem-20 57 102     SPACE eurjchem-20 57 103 126.7 126.7 NUM eurjchem-20 57 104     SPACE eurjchem-20 57 105 ( ( PUNCT eurjchem-20 57 106 c‐3 c‐3 NOUN eurjchem-20 57 107 '' '' PUNCT eurjchem-20 57 108     SPACE eurjchem-20 57 109 & & CCONJ eurjchem-20 57 110     SPACE eurjchem-20 57 111 c‐5 c‐5 NOUN eurjchem-20 57 112 '' '' PUNCT eurjchem-20 57 113 ) ) PUNCT eurjchem-20 57 114 , , PUNCT eurjchem-20 57 115     SPACE eurjchem-20 57 116 125.5 125.5 NUM eurjchem-20 57 117     SPACE eurjchem-20 57 118 ( ( PUNCT eurjchem-20 57 119 c‐2 c‐2 NOUN eurjchem-20 57 120 '' '' PUNCT eurjchem-20 57 121     SPACE eurjchem-20 57 122 & & CCONJ eurjchem-20 57 123     SPACE eurjchem-20 57 124 c‐6 c‐6 NOUN eurjchem-20 57 125 '' '' PUNCT eurjchem-20 57 126 ) ) PUNCT eurjchem-20 57 127 , , PUNCT eurjchem-20 57 128     SPACE eurjchem-20 57 129 110 110 NUM eurjchem-20 57 130     SPACE eurjchem-20 57 131 ( ( PUNCT eurjchem-20 57 132 c‐5 c‐5 NOUN eurjchem-20 57 133 ) ) PUNCT eurjchem-20 57 134 , , PUNCT eurjchem-20 57 135     SPACE eurjchem-20 57 136 89.1 89.1 NUM eurjchem-20 57 137     SPACE eurjchem-20 57 138 ( ( PUNCT eurjchem-20 57 139 c‐1 c‐1 NOUN eurjchem-20 57 140 ' ' PUNCT eurjchem-20 57 141 ) ) PUNCT eurjchem-20 57 142 , , PUNCT eurjchem-20 57 143     SPACE eurjchem-20 57 144 85.8 85.8 NUM eurjchem-20 57 145     SPACE eurjchem-20 57 146 ( ( PUNCT eurjchem-20 57 147 c‐4 c‐4 PROPN eurjchem-20 57 148 ' ' PUNCT eurjchem-20 57 149 ) ) PUNCT eurjchem-20 57 150 , , PUNCT eurjchem-20 57 151     SPACE eurjchem-20 57 152 66.2 66.2 NUM eurjchem-20 57 153     SPACE eurjchem-20 57 154 ( ( PUNCT eurjchem-20 57 155 c‐5 c‐5 NOUN eurjchem-20 57 156 ' ' PUNCT eurjchem-20 57 157 ) ) PUNCT eurjchem-20 57 158 , , PUNCT eurjchem-20 57 159     SPACE eurjchem-20 57 160 58.14 58.14 NUM eurjchem-20 57 161     SPACE eurjchem-20 57 162 ( ( PUNCT eurjchem-20 57 163 o‐ o‐ PROPN eurjchem-20 57 164 ch2‐ch3 ch2‐ch3 PROPN eurjchem-20 57 165 ) ) PUNCT eurjchem-20 57 166 , , PUNCT eurjchem-20 57 167     SPACE eurjchem-20 57 168 45.7 45.7 NUM eurjchem-20 57 169     SPACE eurjchem-20 57 170 ( ( PUNCT eurjchem-20 57 171 gly‐ch gly‐ch PROPN eurjchem-20 57 172 ) ) PUNCT eurjchem-20 57 173 , , PUNCT eurjchem-20 57 174     SPACE eurjchem-20 57 175 12.2 12.2 NUM eurjchem-20 57 176     SPACE eurjchem-20 57 177 ( ( PUNCT eurjchem-20 57 178 o‐ch2‐ch3 o‐ch2‐ch3 ADJ eurjchem-20 57 179 ) ) PUNCT eurjchem-20 57 180 , , PUNCT eurjchem-20 57 181     SPACE eurjchem-20 57 182 11.3 11.3 NUM eurjchem-20 57 183     SPACE eurjchem-20 57 184 ( ( PUNCT eurjchem-20 57 185 ch3 ch3 PROPN eurjchem-20 57 186 ) ) PUNCT eurjchem-20 57 187 . . PUNCT eurjchem-20 57 188     SPACE eurjchem-20 58 1 31p‐nmr 31p‐nmr NOUN eurjchem-20 58 2     SPACE eurjchem-20 58 3 ( ( PUNCT eurjchem-20 58 4 202 202 NUM eurjchem-20 58 5     SPACE eurjchem-20 58 6 mhz mhz NOUN eurjchem-20 58 7 , , PUNCT eurjchem-20 58 8     SPACE eurjchem-20 58 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 58 10 , , PUNCT eurjchem-20 58 11     SPACE eurjchem-20 58 12   NUM eurjchem-20 58 13 ): ): PUNCT eurjchem-20 58 14     SPACE eurjchem-20 58 15 5.78 5.78 NUM eurjchem-20 58 16 . . PUNCT eurjchem-20 58 17     SPACE eurjchem-20 58 18 gcms gcms PROPN eurjchem-20 58 19     SPACE eurjchem-20 58 20 ( ( PUNCT eurjchem-20 58 21 m m PROPN eurjchem-20 58 22 / / SYM eurjchem-20 58 23 z z NOUN eurjchem-20 58 24 ; ; PUNCT eurjchem-20 58 25     SPACE eurjchem-20 58 26 % % NOUN eurjchem-20 58 27 ): ): PUNCT eurjchem-20 58 28     SPACE eurjchem-20 58 29 ( ( PUNCT eurjchem-20 58 30 586.2 586.2 NUM eurjchem-20 58 31 , , PUNCT eurjchem-20 58 32     SPACE eurjchem-20 58 33 35 35 NUM eurjchem-20 58 34 % % NOUN eurjchem-20 58 35 ) ) PUNCT eurjchem-20 58 36     SPACE eurjchem-20 59 1 [ [ X eurjchem-20 59 2 mh]+ mh]+ X eurjchem-20 59 3 . . PUNCT eurjchem-20 59 4           SPACE eurjchem-20 59 5 2.2.6 2.2.6 NUM eurjchem-20 59 6 . . PUNCT eurjchem-20 59 7     SPACE eurjchem-20 59 8 methyl3­(4­hydroxyphenyl)­2­((s)­((5­(5­methyl­2,4­ methyl3­(4­hydroxyphenyl)­2­((s)­((5­(5­methyl­2,4­ ADJ eurjchem-20 59 9 dioxo­3,4­dihydropyrimidin­1(2h)­yl)­2,5­dihydrofuran­2­ dioxo­3,4­dihydropyrimidin­1(2h)­yl)­2,5­dihydrofuran­2­ VERB eurjchem-20 59 10 yl yl NOUN eurjchem-20 59 11 ) ) PUNCT eurjchem-20 59 12     SPACE eurjchem-20 59 13 methoxy)(4­nitrophenoxy)phosphorylamino methoxy)(4­nitrophenoxy)phosphorylamino NOUN eurjchem-20 59 14 ) ) PUNCT eurjchem-20 59 15     SPACE eurjchem-20 59 16 propanoate propanoate NOUN eurjchem-20 59 17     SPACE eurjchem-20 59 18 ( ( PUNCT eurjchem-20 59 19 4f 4f NUM eurjchem-20 59 20 ) ) PUNCT eurjchem-20 59 21         SPACE eurjchem-20 59 22 yield yield NOUN eurjchem-20 59 23 : : PUNCT eurjchem-20 59 24     SPACE eurjchem-20 59 25 62 62 NUM eurjchem-20 59 26 % % NOUN eurjchem-20 59 27 . . PUNCT eurjchem-20 59 28     SPACE eurjchem-20 60 1 m.p m.p PROPN eurjchem-20 60 2 . . PROPN eurjchem-20 60 3 : : PUNCT eurjchem-20 60 4     SPACE eurjchem-20 60 5 154‐156 154‐156 NOUN eurjchem-20 60 6     SPACE eurjchem-20 60 7 oc oc PROPN eurjchem-20 60 8     SPACE eurjchem-20 60 9 ir ir VERB eurjchem-20 60 10     SPACE eurjchem-20 60 11 ( ( PUNCT eurjchem-20 60 12 kbr kbr PROPN eurjchem-20 60 13 , , PUNCT eurjchem-20 60 14     SPACE eurjchem-20 60 15 cm‐1 cm‐1 NOUN eurjchem-20 60 16 ): ): PUNCT eurjchem-20 60 17     SPACE eurjchem-20 60 18 3378 3378 NUM eurjchem-20 60 19     SPACE eurjchem-20 60 20 ν(‐nh ν(‐nh PROPN eurjchem-20 60 21 ) ) PUNCT eurjchem-20 60 22 , , PUNCT eurjchem-20 60 23     SPACE eurjchem-20 60 24 1678 1678 NUM eurjchem-20 60 25 , , PUNCT eurjchem-20 60 26     SPACE eurjchem-20 60 27 1723 1723 NUM eurjchem-20 60 28     SPACE eurjchem-20 60 29 ν(c ν(c PROPN eurjchem-20 60 30 = = NOUN eurjchem-20 60 31 o o NOUN eurjchem-20 60 32 ) ) PUNCT eurjchem-20 60 33 , , PUNCT eurjchem-20 60 34     SPACE eurjchem-20 60 35 1218 1218 NUM eurjchem-20 60 36     SPACE eurjchem-20 60 37 ν(p ν(p PROPN eurjchem-20 60 38 = = SYM eurjchem-20 60 39 o o NOUN eurjchem-20 60 40 ) ) PUNCT eurjchem-20 60 41 . . PUNCT eurjchem-20 60 42     SPACE eurjchem-20 61 1 1h‐nmr 1h‐nmr NUM eurjchem-20 61 2     SPACE eurjchem-20 61 3 ( ( PUNCT eurjchem-20 61 4 500 500 NUM eurjchem-20 61 5     SPACE eurjchem-20 61 6 mhz mhz NOUN eurjchem-20 61 7 , , PUNCT eurjchem-20 61 8     SPACE eurjchem-20 61 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 61 10 , , PUNCT eurjchem-20 61 11     SPACE eurjchem-20 61 12   NUM eurjchem-20 61 13 ): ): PUNCT eurjchem-20 61 14     SPACE eurjchem-20 61 15 8.5 8.5 NUM eurjchem-20 61 16     SPACE eurjchem-20 61 17 ( ( PUNCT eurjchem-20 61 18 s s PROPN eurjchem-20 61 19 , , PUNCT eurjchem-20 61 20     SPACE eurjchem-20 61 21 1h 1h NUM eurjchem-20 61 22 , , PUNCT eurjchem-20 61 23     SPACE eurjchem-20 61 24 nh nh PROPN eurjchem-20 61 25 ) ) PUNCT eurjchem-20 61 26 , , PUNCT eurjchem-20 61 27     SPACE eurjchem-20 61 28 7.92 7.92 NUM eurjchem-20 61 29     SPACE eurjchem-20 61 30 ( ( PUNCT eurjchem-20 61 31 d d NOUN eurjchem-20 61 32 , , PUNCT eurjchem-20 61 33     SPACE eurjchem-20 61 34 2h 2h NUM eurjchem-20 61 35 , , PUNCT eurjchem-20 61 36     SPACE eurjchem-20 61 37 j=9.5 j=9.5 NOUN eurjchem-20 61 38     SPACE eurjchem-20 61 39 hz hz VERB eurjchem-20 61 40 , , PUNCT eurjchem-20 61 41     SPACE eurjchem-20 61 42 ar‐h ar‐h NOUN eurjchem-20 61 43 ) ) PUNCT eurjchem-20 61 44 , , PUNCT eurjchem-20 61 45     SPACE eurjchem-20 61 46 7.49 7.49 NUM eurjchem-20 61 47     SPACE eurjchem-20 61 48 ( ( PUNCT eurjchem-20 61 49 d d PROPN eurjchem-20 61 50 , , PUNCT eurjchem-20 61 51     SPACE eurjchem-20 61 52 1h 1h NUM eurjchem-20 61 53 , , PUNCT eurjchem-20 61 54     SPACE eurjchem-20 61 55 j=1.5 j=1.5 NOUN eurjchem-20 61 56     SPACE eurjchem-20 61 57 hz hz VERB eurjchem-20 61 58 , , PUNCT eurjchem-20 61 59     SPACE eurjchem-20 61 60 h‐6 h‐6 NOUN eurjchem-20 61 61 ) ) PUNCT eurjchem-20 61 62 , , PUNCT eurjchem-20 61 63     SPACE eurjchem-20 61 64 7.38 7.38 NUM eurjchem-20 61 65     SPACE eurjchem-20 61 66 ( ( PUNCT eurjchem-20 61 67 d d NOUN eurjchem-20 61 68 , , PUNCT eurjchem-20 61 69     SPACE eurjchem-20 61 70 2h 2h NUM eurjchem-20 61 71 , , PUNCT eurjchem-20 61 72     SPACE eurjchem-20 62 1 j=9 j=9 NOUN eurjchem-20 62 2     SPACE eurjchem-20 62 3 hz hz VERB eurjchem-20 62 4 , , PUNCT eurjchem-20 62 5     SPACE eurjchem-20 62 6 ar‐h ar‐h NOUN eurjchem-20 62 7 ) ) PUNCT eurjchem-20 62 8 , , PUNCT eurjchem-20 62 9     SPACE eurjchem-20 62 10 7.15 7.15 NUM eurjchem-20 62 11     SPACE eurjchem-20 62 12 ( ( PUNCT eurjchem-20 62 13 d d NOUN eurjchem-20 62 14 , , PUNCT eurjchem-20 62 15     SPACE eurjchem-20 62 16 2h 2h NUM eurjchem-20 62 17 , , PUNCT eurjchem-20 62 18     SPACE eurjchem-20 62 19 j=8.5 j=8.5 PROPN eurjchem-20 62 20     SPACE eurjchem-20 62 21 hz hz VERB eurjchem-20 62 22 , , PUNCT eurjchem-20 62 23     SPACE eurjchem-20 62 24 ar‐h ar‐h NOUN eurjchem-20 62 25 ) ) PUNCT eurjchem-20 62 26 , , PUNCT eurjchem-20 62 27     SPACE eurjchem-20 62 28 6.89 6.89 NUM eurjchem-20 62 29     SPACE eurjchem-20 62 30 ( ( PUNCT eurjchem-20 62 31 d d NOUN eurjchem-20 62 32 , , PUNCT eurjchem-20 62 33     SPACE eurjchem-20 62 34 2h 2h NUM eurjchem-20 62 35 , , PUNCT eurjchem-20 62 36     SPACE eurjchem-20 62 37 j=9 j=9 NOUN eurjchem-20 62 38     SPACE eurjchem-20 62 39 hz hz VERB eurjchem-20 62 40 , , PUNCT eurjchem-20 62 41     SPACE eurjchem-20 62 42 ar‐h ar‐h NOUN eurjchem-20 62 43 ) ) PUNCT eurjchem-20 62 44 , , PUNCT eurjchem-20 62 45     SPACE eurjchem-20 63 1 6.78‐6.79 6.78‐6.79 NOUN eurjchem-20 63 2     SPACE eurjchem-20 63 3 ( ( PUNCT eurjchem-20 63 4 m m PROPN eurjchem-20 63 5 , , PUNCT eurjchem-20 63 6     SPACE eurjchem-20 63 7 1h 1h NUM eurjchem-20 63 8 , , PUNCT eurjchem-20 63 9     SPACE eurjchem-20 63 10 h‐1 h‐1 PROPN eurjchem-20 63 11 ' ' PUNCT eurjchem-20 63 12 ) ) PUNCT eurjchem-20 63 13 , , PUNCT eurjchem-20 63 14     SPACE eurjchem-20 63 15 6.3‐6.32 6.3‐6.32 NUM eurjchem-20 63 16     SPACE eurjchem-20 63 17 ( ( PUNCT eurjchem-20 63 18 m m PROPN eurjchem-20 63 19 , , PUNCT eurjchem-20 63 20     SPACE eurjchem-20 63 21 1h 1h NUM eurjchem-20 63 22 , , PUNCT eurjchem-20 63 23     SPACE eurjchem-20 63 24 h‐2 h‐2 NOUN eurjchem-20 63 25 ' ' PUNCT eurjchem-20 63 26 ) ) PUNCT eurjchem-20 63 27 , , PUNCT eurjchem-20 63 28     SPACE eurjchem-20 63 29 5.87‐5.89 5.87‐5.89 NOUN eurjchem-20 63 30     SPACE eurjchem-20 63 31 ( ( PUNCT eurjchem-20 63 32 m m PROPN eurjchem-20 63 33 , , PUNCT eurjchem-20 63 34     SPACE eurjchem-20 63 35 1h 1h NUM eurjchem-20 63 36 , , PUNCT eurjchem-20 63 37     SPACE eurjchem-20 63 38 h‐3 h‐3 NOUN eurjchem-20 63 39 ' ' PUNCT eurjchem-20 63 40 ) ) PUNCT eurjchem-20 63 41 , , PUNCT eurjchem-20 63 42     SPACE eurjchem-20 63 43 5.47 5.47 NUM eurjchem-20 63 44     SPACE eurjchem-20 63 45 ( ( PUNCT eurjchem-20 63 46 s s PROPN eurjchem-20 63 47 , , PUNCT eurjchem-20 63 48     SPACE eurjchem-20 63 49 1h 1h NUM eurjchem-20 63 50 , , PUNCT eurjchem-20 63 51     SPACE eurjchem-20 63 52 tyr‐oh tyr‐oh NOUN eurjchem-20 63 53 ) ) PUNCT eurjchem-20 63 54 , , PUNCT eurjchem-20 63 55     SPACE eurjchem-20 63 56 4.7 4.7 NUM eurjchem-20 63 57     SPACE eurjchem-20 63 58 ( ( PUNCT eurjchem-20 63 59 brs br VERB eurjchem-20 63 60 , , PUNCT eurjchem-20 63 61     SPACE eurjchem-20 63 62 1h 1h NUM eurjchem-20 63 63 , , PUNCT eurjchem-20 63 64     SPACE eurjchem-20 63 65 tyr‐nh tyr‐nh PROPN eurjchem-20 63 66 ) ) PUNCT eurjchem-20 63 67 , , PUNCT eurjchem-20 63 68     SPACE eurjchem-20 63 69 3.91‐3.97 3.91‐3.97 NOUN eurjchem-20 63 70     SPACE eurjchem-20 63 71 ( ( PUNCT eurjchem-20 63 72 m m PROPN eurjchem-20 63 73 , , PUNCT eurjchem-20 63 74     SPACE eurjchem-20 63 75 4h 4h NOUN eurjchem-20 63 76 , , PUNCT eurjchem-20 63 77     SPACE eurjchem-20 63 78 2h‐5 2h‐5 NUM eurjchem-20 63 79 ' ' PUNCT eurjchem-20 63 80 , , PUNCT eurjchem-20 63 81     SPACE eurjchem-20 63 82 h‐4 h‐4 NOUN eurjchem-20 63 83 ' ' PUNCT eurjchem-20 63 84 , , PUNCT eurjchem-20 63 85     SPACE eurjchem-20 63 86 tyr‐nh‐ch tyr‐nh‐ch NUM eurjchem-20 63 87 ) ) PUNCT eurjchem-20 63 88 , , PUNCT eurjchem-20 63 89     SPACE eurjchem-20 63 90 3.51‐ 3.51‐ NUM eurjchem-20 63 91 3.53 3.53 NUM eurjchem-20 63 92     SPACE eurjchem-20 63 93 ( ( PUNCT eurjchem-20 63 94 m m PROPN eurjchem-20 63 95 , , PUNCT eurjchem-20 63 96     SPACE eurjchem-20 63 97 2h 2h NUM eurjchem-20 63 98 , , PUNCT eurjchem-20 63 99     SPACE eurjchem-20 63 100 tyr‐ch2 tyr‐ch2 NOUN eurjchem-20 63 101 ) ) PUNCT eurjchem-20 63 102 , , PUNCT eurjchem-20 63 103     SPACE eurjchem-20 63 104 3.32 3.32 NUM eurjchem-20 63 105     SPACE eurjchem-20 63 106 ( ( PUNCT eurjchem-20 63 107 s s PROPN eurjchem-20 63 108 , , PUNCT eurjchem-20 63 109     SPACE eurjchem-20 63 110 3h 3h NUM eurjchem-20 63 111 , , PUNCT eurjchem-20 63 112     SPACE eurjchem-20 63 113 ‐och3 ‐och3 NOUN eurjchem-20 63 114 ) ) PUNCT eurjchem-20 63 115 , , PUNCT eurjchem-20 63 116     SPACE eurjchem-20 63 117 4.71 4.71 NUM eurjchem-20 63 118     SPACE eurjchem-20 63 119 ( ( PUNCT eurjchem-20 63 120 s s PROPN eurjchem-20 63 121 , , PUNCT eurjchem-20 63 122     SPACE eurjchem-20 63 123 3h 3h NUM eurjchem-20 63 124 , , PUNCT eurjchem-20 63 125     SPACE eurjchem-20 63 126 ch3 ch3 PROPN eurjchem-20 63 127 ) ) PUNCT eurjchem-20 63 128 , , PUNCT eurjchem-20 63 129     SPACE eurjchem-20 63 130 31p‐ 31p‐ NUM eurjchem-20 63 131 nmr nmr NOUN eurjchem-20 63 132     SPACE eurjchem-20 63 133 ( ( PUNCT eurjchem-20 63 134 202 202 NUM eurjchem-20 63 135     SPACE eurjchem-20 63 136 mhz mhz NOUN eurjchem-20 63 137 , , PUNCT eurjchem-20 63 138     SPACE eurjchem-20 63 139 dmso‐d6 dmso‐d6 NOUN eurjchem-20 63 140 , , PUNCT eurjchem-20 63 141     SPACE eurjchem-20 63 142   NUM eurjchem-20 63 143 ): ): PUNCT eurjchem-20 63 144     SPACE eurjchem-20 63 145 5.91 5.91 NUM eurjchem-20 63 146 , , PUNCT eurjchem-20 63 147     SPACE eurjchem-20 63 148 6.54 6.54 NUM eurjchem-20 63 149 . . PUNCT eurjchem-20 63 150         SPACE eurjchem-20 64 1 2.2.7 2.2.7 X eurjchem-20 64 2 . . PUNCT eurjchem-20 64 3     SPACE eurjchem-20 64 4 ethyl2­(4­hydroxyphenyl)­2­((s)­((5­(5­methyl­2,4­ ethyl2­(4­hydroxyphenyl)­2­((s)­((5­(5­methyl­2,4­ ADJ eurjchem-20 64 5 dioxo­3,4­dihydropyrimidin­1(2h)­yl)­2,5­dihydrofuran­2­ dioxo­3,4­dihydropyrimidin­1(2h)­yl)­2,5­dihydrofuran­2­ VERB eurjchem-20 64 6 yl yl NOUN eurjchem-20 64 7 ) ) PUNCT eurjchem-20 64 8     SPACE eurjchem-20 64 9 methoxy methoxy NOUN eurjchem-20 64 10 ) ) PUNCT eurjchem-20 64 11     SPACE eurjchem-20 64 12 ( ( PUNCT eurjchem-20 64 13 4­nitrophenoxy)phosphorylamino)acetate 4­nitrophenoxy)phosphorylamino)acetate ADJ eurjchem-20 64 14     SPACE eurjchem-20 64 15 ( ( PUNCT eurjchem-20 64 16 4 4 NUM eurjchem-20 64 17 g g NOUN eurjchem-20 64 18 ) ) PUNCT eurjchem-20 64 19         SPACE eurjchem-20 64 20 yield yield NOUN eurjchem-20 64 21 : : PUNCT eurjchem-20 64 22     SPACE eurjchem-20 64 23 57 57 NUM eurjchem-20 64 24 % % NOUN eurjchem-20 64 25 . . PUNCT eurjchem-20 64 26     SPACE eurjchem-20 65 1 m.p m.p PROPN eurjchem-20 65 2 . . PROPN eurjchem-20 65 3 : : PUNCT eurjchem-20 65 4     SPACE eurjchem-20 65 5 167‐169 167‐169 NUM eurjchem-20 65 6     SPACE eurjchem-20 65 7 oc oc PROPN eurjchem-20 65 8 , , PUNCT eurjchem-20 65 9     SPACE eurjchem-20 65 10 anal anal ADJ eurjchem-20 65 11 . . PUNCT eurjchem-20 65 12     SPACE eurjchem-20 65 13 calcd calcd NOUN eurjchem-20 65 14 . . PUNCT eurjchem-20 65 15     SPACE eurjchem-20 65 16 for for ADP eurjchem-20 65 17     SPACE eurjchem-20 65 18 c26h27n4o11p c26h27n4o11p NUM eurjchem-20 65 19 : : PUNCT eurjchem-20 65 20     SPACE eurjchem-20 65 21 c c X eurjchem-20 65 22 , , PUNCT eurjchem-20 65 23     SPACE eurjchem-20 65 24 51.83 51.83 NUM eurjchem-20 65 25 ; ; PUNCT eurjchem-20 65 26     SPACE eurjchem-20 65 27 h h NOUN eurjchem-20 65 28 , , PUNCT eurjchem-20 65 29     SPACE eurjchem-20 65 30 4.52 4.52 NUM eurjchem-20 65 31 ; ; PUNCT eurjchem-20 65 32     SPACE eurjchem-20 65 33 n n CCONJ eurjchem-20 65 34 , , PUNCT eurjchem-20 65 35     SPACE eurjchem-20 65 36 9.30 9.30 NUM eurjchem-20 65 37 ; ; PUNCT eurjchem-20 65 38     SPACE eurjchem-20 65 39 found find VERB eurjchem-20 65 40     SPACE eurjchem-20 65 41 c c NOUN eurjchem-20 65 42 , , PUNCT eurjchem-20 65 43     SPACE eurjchem-20 65 44 51.79 51.79 NUM eurjchem-20 65 45 ; ; PUNCT eurjchem-20 65 46     SPACE eurjchem-20 65 47 h h NOUN eurjchem-20 65 48 , , PUNCT eurjchem-20 65 49     SPACE eurjchem-20 65 50 4.47 4.47 NUM eurjchem-20 65 51 ; ; PUNCT eurjchem-20 65 52     SPACE eurjchem-20 65 53 n n CCONJ eurjchem-20 65 54 , , PUNCT eurjchem-20 65 55     SPACE eurjchem-20 65 56 9.35 9.35 NUM eurjchem-20 65 57 . . PUNCT eurjchem-20 65 58     SPACE eurjchem-20 66 1 ir ir PROPN eurjchem-20 66 2     SPACE eurjchem-20 66 3 ( ( PUNCT eurjchem-20 66 4 kbr kbr PROPN eurjchem-20 66 5 , , PUNCT eurjchem-20 66 6     SPACE eurjchem-20 66 7 cm‐1 cm‐1 NOUN eurjchem-20 66 8 ): ): PUNCT eurjchem-20 66 9     SPACE eurjchem-20 66 10 3385 3385 NUM eurjchem-20 66 11     SPACE eurjchem-20 66 12 ν(‐nh ν(‐nh PROPN eurjchem-20 66 13 ) ) PUNCT eurjchem-20 66 14 , , PUNCT eurjchem-20 66 15     SPACE eurjchem-20 66 16 1683 1683 NUM eurjchem-20 66 17 , , PUNCT eurjchem-20 66 18     SPACE eurjchem-20 66 19 1725 1725 NUM eurjchem-20 66 20     SPACE eurjchem-20 66 21 ν(c ν(c PROPN eurjchem-20 66 22 = = SYM eurjchem-20 66 23 o o NOUN eurjchem-20 66 24 ) ) PUNCT eurjchem-20 66 25 , , PUNCT eurjchem-20 66 26     SPACE eurjchem-20 66 27 1230 1230 NUM eurjchem-20 66 28     SPACE eurjchem-20 66 29 ν(p ν(p PROPN eurjchem-20 66 30 = = SYM eurjchem-20 66 31 o o NOUN eurjchem-20 66 32 ) ) PUNCT eurjchem-20 66 33 . . PUNCT eurjchem-20 66 34     SPACE eurjchem-20 67 1 1h‐ 1h‐ NUM eurjchem-20 67 2 nmr nmr PROPN eurjchem-20 67 3     SPACE eurjchem-20 67 4 ( ( PUNCT eurjchem-20 67 5 500 500 NUM eurjchem-20 67 6     SPACE eurjchem-20 67 7 mhz mhz NOUN eurjchem-20 67 8 , , PUNCT eurjchem-20 67 9     SPACE eurjchem-20 67 10 dmso‐d6 dmso‐d6 NOUN eurjchem-20 67 11 , , PUNCT eurjchem-20 67 12     SPACE eurjchem-20 67 13   NUM eurjchem-20 67 14 ): ): PUNCT eurjchem-20 67 15     SPACE eurjchem-20 67 16 11.1 11.1 NUM eurjchem-20 67 17     SPACE eurjchem-20 67 18 ( ( PUNCT eurjchem-20 67 19 s s PROPN eurjchem-20 67 20 , , PUNCT eurjchem-20 67 21     SPACE eurjchem-20 67 22 1h 1h NUM eurjchem-20 67 23 , , PUNCT eurjchem-20 67 24     SPACE eurjchem-20 67 25 nh nh PROPN eurjchem-20 67 26 ) ) PUNCT eurjchem-20 67 27 , , PUNCT eurjchem-20 67 28     SPACE eurjchem-20 67 29 8.18 8.18 NUM eurjchem-20 67 30     SPACE eurjchem-20 67 31 ( ( PUNCT eurjchem-20 67 32 d d NOUN eurjchem-20 67 33 , , PUNCT eurjchem-20 67 34     SPACE eurjchem-20 67 35 2h 2h NUM eurjchem-20 67 36 , , PUNCT eurjchem-20 67 37     SPACE eurjchem-20 67 38 j=9 j=9 NOUN eurjchem-20 67 39     SPACE eurjchem-20 67 40 hz hz VERB eurjchem-20 67 41 , , PUNCT eurjchem-20 67 42     SPACE eurjchem-20 67 43 ar‐h ar‐h NOUN eurjchem-20 67 44 ) ) PUNCT eurjchem-20 67 45 , , PUNCT eurjchem-20 67 46     SPACE eurjchem-20 67 47 8.11 8.11 NUM eurjchem-20 67 48     SPACE eurjchem-20 67 49 ( ( PUNCT eurjchem-20 67 50 d d NOUN eurjchem-20 67 51 , , PUNCT eurjchem-20 67 52     SPACE eurjchem-20 67 53 2h 2h NUM eurjchem-20 67 54 , , PUNCT eurjchem-20 67 55     SPACE eurjchem-20 67 56 j=9.5 j=9.5 NOUN eurjchem-20 67 57     SPACE eurjchem-20 67 58 hz hz VERB eurjchem-20 67 59 , , PUNCT eurjchem-20 67 60     SPACE eurjchem-20 67 61 ar‐h ar‐h NOUN eurjchem-20 67 62 ) ) PUNCT eurjchem-20 67 63 , , PUNCT eurjchem-20 67 64     SPACE eurjchem-20 67 65 7.51 7.51 NUM eurjchem-20 67 66     SPACE eurjchem-20 67 67 ( ( PUNCT eurjchem-20 67 68 d d PROPN eurjchem-20 67 69 , , PUNCT eurjchem-20 67 70     SPACE eurjchem-20 67 71 1h 1h NUM eurjchem-20 67 72 , , PUNCT eurjchem-20 67 73     SPACE eurjchem-20 67 74 j=1.5 j=1.5 NOUN eurjchem-20 67 75     SPACE eurjchem-20 67 76 hz hz VERB eurjchem-20 67 77 , , PUNCT eurjchem-20 67 78     SPACE eurjchem-20 67 79 h‐ h‐ PROPN eurjchem-20 67 80 6 6 NUM eurjchem-20 67 81 ) ) PUNCT eurjchem-20 67 82 , , PUNCT eurjchem-20 67 83     SPACE eurjchem-20 68 1 7.25‐7.43 7.25‐7.43 NOUN eurjchem-20 68 2     SPACE eurjchem-20 68 3 ( ( PUNCT eurjchem-20 68 4 m m PROPN eurjchem-20 68 5 , , PUNCT eurjchem-20 68 6     SPACE eurjchem-20 68 7 5h 5h NUM eurjchem-20 68 8 , , PUNCT eurjchem-20 68 9     SPACE eurjchem-20 68 10 ar‐h ar‐h NOUN eurjchem-20 68 11 ) ) PUNCT eurjchem-20 68 12 , , PUNCT eurjchem-20 68 13     SPACE eurjchem-20 68 14 6.79‐6.81 6.79‐6.81 NUM eurjchem-20 68 15     SPACE eurjchem-20 68 16 ( ( PUNCT eurjchem-20 68 17 m m PROPN eurjchem-20 68 18 , , PUNCT eurjchem-20 68 19     SPACE eurjchem-20 68 20 1h 1h NUM eurjchem-20 68 21 , , PUNCT eurjchem-20 68 22     SPACE eurjchem-20 68 23 h‐1 h‐1 PROPN eurjchem-20 68 24 ' ' PUNCT eurjchem-20 68 25 ) ) PUNCT eurjchem-20 68 26 , , PUNCT eurjchem-20 68 27     SPACE eurjchem-20 68 28 6.29‐6.31 6.29‐6.31 NUM eurjchem-20 68 29     SPACE eurjchem-20 68 30 ( ( PUNCT eurjchem-20 68 31 m m PROPN eurjchem-20 68 32 , , PUNCT eurjchem-20 68 33     SPACE eurjchem-20 68 34 1h 1h NUM eurjchem-20 68 35 , , PUNCT eurjchem-20 68 36     SPACE eurjchem-20 68 37 h‐2 h‐2 NOUN eurjchem-20 68 38 ' ' PUNCT eurjchem-20 68 39 ) ) PUNCT eurjchem-20 68 40 , , PUNCT eurjchem-20 68 41     SPACE eurjchem-20 68 42 5.87‐5.89 5.87‐5.89 NOUN eurjchem-20 68 43     SPACE eurjchem-20 68 44 ( ( PUNCT eurjchem-20 68 45 m m PROPN eurjchem-20 68 46 , , PUNCT eurjchem-20 68 47     SPACE eurjchem-20 68 48 1h 1h NUM eurjchem-20 68 49 , , PUNCT eurjchem-20 68 50     SPACE eurjchem-20 68 51 h‐3 h‐3 NOUN eurjchem-20 68 52 ' ' PUNCT eurjchem-20 68 53 ) ) PUNCT eurjchem-20 68 54 , , PUNCT eurjchem-20 68 55     SPACE eurjchem-20 68 56 5.54 5.54 NUM eurjchem-20 68 57     SPACE eurjchem-20 68 58 ( ( PUNCT eurjchem-20 68 59 s s PROPN eurjchem-20 68 60 , , PUNCT eurjchem-20 68 61     SPACE eurjchem-20 68 62 1h 1h NUM eurjchem-20 68 63 , , PUNCT eurjchem-20 68 64     SPACE eurjchem-20 68 65 gly‐oh gly‐oh NOUN eurjchem-20 68 66 ) ) PUNCT eurjchem-20 68 67 , , PUNCT eurjchem-20 68 68     SPACE eurjchem-20 68 69 4.4 4.4 NUM eurjchem-20 68 70     SPACE eurjchem-20 68 71 ( ( PUNCT eurjchem-20 68 72 brs br VERB eurjchem-20 68 73 , , PUNCT eurjchem-20 68 74     SPACE eurjchem-20 68 75 1h 1h NUM eurjchem-20 68 76 , , PUNCT eurjchem-20 68 77     SPACE eurjchem-20 68 78 gly‐nh gly‐nh PROPN eurjchem-20 68 79 ) ) PUNCT eurjchem-20 68 80 , , PUNCT eurjchem-20 68 81     SPACE eurjchem-20 68 82 3.55‐3.61 3.55‐3.61 NOUN eurjchem-20 68 83     SPACE eurjchem-20 68 84 ( ( PUNCT eurjchem-20 68 85 m m PROPN eurjchem-20 68 86 , , PUNCT eurjchem-20 68 87     SPACE eurjchem-20 68 88 4h 4h NOUN eurjchem-20 68 89 , , PUNCT eurjchem-20 68 90     SPACE eurjchem-20 68 91 2h‐5 2h‐5 NUM eurjchem-20 68 92 ' ' PUNCT eurjchem-20 68 93 , , PUNCT eurjchem-20 68 94     SPACE eurjchem-20 68 95 h‐4 h‐4 NOUN eurjchem-20 68 96 ' ' PART eurjchem-20 68 97 , , PUNCT eurjchem-20 68 98     SPACE eurjchem-20 68 99 gly‐nh‐ch gly‐nh‐ch NOUN eurjchem-20 68 100 ) ) PUNCT eurjchem-20 68 101 , , PUNCT eurjchem-20 68 102     SPACE eurjchem-20 68 103 3.11 3.11 NUM eurjchem-20 68 104     SPACE eurjchem-20 68 105 ( ( PUNCT eurjchem-20 68 106 q q NOUN eurjchem-20 68 107 , , PUNCT eurjchem-20 68 108     SPACE eurjchem-20 68 109 2h 2h NUM eurjchem-20 68 110 , , PUNCT eurjchem-20 68 111     SPACE eurjchem-20 68 112 ‐och2 ‐och2 NOUN eurjchem-20 68 113 ) ) PUNCT eurjchem-20 68 114 , , PUNCT eurjchem-20 68 115     SPACE eurjchem-20 68 116 1.71 1.71 NUM eurjchem-20 68 117     SPACE eurjchem-20 68 118 ( ( PUNCT eurjchem-20 68 119 s s PROPN eurjchem-20 68 120 , , PUNCT eurjchem-20 68 121     SPACE eurjchem-20 68 122 3h 3h NUM eurjchem-20 68 123 , , PUNCT eurjchem-20 68 124     SPACE eurjchem-20 68 125 ch3 ch3 PROPN eurjchem-20 68 126 ) ) PUNCT eurjchem-20 68 127 , , PUNCT eurjchem-20 68 128     SPACE eurjchem-20 68 129 1.21 1.21 NUM eurjchem-20 68 130     SPACE eurjchem-20 68 131 ( ( PUNCT eurjchem-20 68 132 t t PROPN eurjchem-20 68 133 , , PUNCT eurjchem-20 68 134     SPACE eurjchem-20 68 135 3h 3h NUM eurjchem-20 68 136 , , PUNCT eurjchem-20 68 137     SPACE eurjchem-20 68 138 o‐ch2‐ch3 o‐ch2‐ch3 ADJ eurjchem-20 68 139 ) ) PUNCT eurjchem-20 68 140 . . PUNCT eurjchem-20 68 141     SPACE eurjchem-20 69 1 31p‐nmr 31p‐nmr NOUN eurjchem-20 69 2     SPACE eurjchem-20 69 3 ( ( PUNCT eurjchem-20 69 4 202 202 NUM eurjchem-20 69 5     SPACE eurjchem-20 69 6 mhz mhz NOUN eurjchem-20 69 7 , , PUNCT eurjchem-20 69 8     SPACE eurjchem-20 69 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 69 10 , , PUNCT eurjchem-20 69 11     SPACE eurjchem-20 69 12   NUM eurjchem-20 69 13 ): ): PUNCT eurjchem-20 69 14     SPACE eurjchem-20 69 15 4.24 4.24 NUM eurjchem-20 69 16 . . PUNCT eurjchem-20 69 17         SPACE eurjchem-20 69 18 2.2.8 2.2.8 NUM eurjchem-20 69 19 . . PUNCT eurjchem-20 69 20     SPACE eurjchem-20 69 21 ( ( PUNCT eurjchem-20 69 22 2s)­methyl­3­methyl­2­((s)­((5­(5­methyl­2,4­dioxo­ 2s)­methyl­3­methyl­2­((s)­((5­(5­methyl­2,4­dioxo­ NUM eurjchem-20 69 23 3,4­dihydropyrimidin­1(2h)­yl)­2,5­dihydrofuran­2­yl 3,4­dihydropyrimidin­1(2h)­yl)­2,5­dihydrofuran­2­yl NUM eurjchem-20 69 24 ) ) PUNCT eurjchem-20 69 25     SPACE eurjchem-20 69 26 met­ met­ PROPN eurjchem-20 69 27 hoxy hoxy PROPN eurjchem-20 69 28 ) ) PUNCT eurjchem-20 69 29     SPACE eurjchem-20 69 30 ( ( PUNCT eurjchem-20 69 31 4­nitrophenoxy)phosphorylamino)butanoate 4­nitrophenoxy)phosphorylamino)butanoate NOUN eurjchem-20 69 32     SPACE eurjchem-20 69 33 ( ( PUNCT eurjchem-20 69 34 4h 4h NOUN eurjchem-20 69 35 ) ) PUNCT eurjchem-20 69 36         SPACE eurjchem-20 69 37 yield yield NOUN eurjchem-20 69 38 : : PUNCT eurjchem-20 69 39     SPACE eurjchem-20 69 40 59 59 NUM eurjchem-20 69 41 % % NOUN eurjchem-20 69 42 . . PUNCT eurjchem-20 69 43     SPACE eurjchem-20 70 1 m.p m.p PROPN eurjchem-20 70 2 . . PROPN eurjchem-20 70 3 : : PUNCT eurjchem-20 70 4     SPACE eurjchem-20 70 5 145‐147 145‐147 NOUN eurjchem-20 70 6     SPACE eurjchem-20 70 7 oc oc PROPN eurjchem-20 70 8     SPACE eurjchem-20 70 9 ir ir VERB eurjchem-20 70 10     SPACE eurjchem-20 70 11 ( ( PUNCT eurjchem-20 70 12 kbr kbr PROPN eurjchem-20 70 13 , , PUNCT eurjchem-20 70 14     SPACE eurjchem-20 70 15 cm‐1 cm‐1 NOUN eurjchem-20 70 16 ): ): PUNCT eurjchem-20 70 17     SPACE eurjchem-20 70 18 3386 3386 NUM eurjchem-20 70 19     SPACE eurjchem-20 70 20 ν(‐nh ν(‐nh PROPN eurjchem-20 70 21 ) ) PUNCT eurjchem-20 70 22 , , PUNCT eurjchem-20 70 23     SPACE eurjchem-20 70 24 1678 1678 NUM eurjchem-20 70 25 , , PUNCT eurjchem-20 70 26     SPACE eurjchem-20 70 27 1731 1731 NUM eurjchem-20 70 28     SPACE eurjchem-20 70 29 ν(c ν(c PROPN eurjchem-20 70 30 = = SYM eurjchem-20 70 31 o o NOUN eurjchem-20 70 32 ) ) PUNCT eurjchem-20 70 33 , , PUNCT eurjchem-20 70 34     SPACE eurjchem-20 70 35 1220 1220 NUM eurjchem-20 70 36     SPACE eurjchem-20 70 37 ν(p ν(p PROPN eurjchem-20 70 38 = = SYM eurjchem-20 70 39 o o NOUN eurjchem-20 70 40 ) ) PUNCT eurjchem-20 70 41 . . PUNCT eurjchem-20 70 42     SPACE eurjchem-20 71 1 1h‐nmr 1h‐nmr NUM eurjchem-20 71 2     SPACE eurjchem-20 71 3 ( ( PUNCT eurjchem-20 71 4 500 500 NUM eurjchem-20 71 5     SPACE eurjchem-20 71 6 mhz mhz NOUN eurjchem-20 71 7 , , PUNCT eurjchem-20 71 8     SPACE eurjchem-20 71 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 71 10 , , PUNCT eurjchem-20 71 11     SPACE eurjchem-20 71 12   NUM eurjchem-20 71 13 ): ): PUNCT eurjchem-20 71 14     SPACE eurjchem-20 71 15 8.1(s 8.1(s NUM eurjchem-20 71 16 , , PUNCT eurjchem-20 71 17     SPACE eurjchem-20 71 18 1h 1h NUM eurjchem-20 71 19 , , PUNCT eurjchem-20 71 20     SPACE eurjchem-20 71 21 nh nh PROPN eurjchem-20 71 22 ) ) PUNCT eurjchem-20 71 23 , , PUNCT eurjchem-20 71 24     SPACE eurjchem-20 71 25 8.0 8.0 NUM eurjchem-20 71 26     SPACE eurjchem-20 71 27 ( ( PUNCT eurjchem-20 71 28 d d PROPN eurjchem-20 71 29 , , PUNCT eurjchem-20 71 30     SPACE eurjchem-20 71 31 2h 2h NUM eurjchem-20 71 32 , , PUNCT eurjchem-20 71 33     SPACE eurjchem-20 71 34 j=9 j=9 NOUN eurjchem-20 71 35     SPACE eurjchem-20 71 36 hz hz VERB eurjchem-20 71 37 , , PUNCT eurjchem-20 71 38     SPACE eurjchem-20 71 39 ar‐h ar‐h NOUN eurjchem-20 71 40 ) ) PUNCT eurjchem-20 71 41 , , PUNCT eurjchem-20 71 42     SPACE eurjchem-20 71 43 7.51 7.51 NUM eurjchem-20 71 44     SPACE eurjchem-20 71 45 ( ( PUNCT eurjchem-20 71 46 d d PROPN eurjchem-20 71 47 , , PUNCT eurjchem-20 71 48     SPACE eurjchem-20 71 49 1h 1h NUM eurjchem-20 71 50 , , PUNCT eurjchem-20 71 51     SPACE eurjchem-20 71 52 j=1 j=1 NOUN eurjchem-20 71 53     SPACE eurjchem-20 71 54 hz hz VERB eurjchem-20 71 55 , , PUNCT eurjchem-20 71 56     SPACE eurjchem-20 71 57 h‐6 h‐6 NOUN eurjchem-20 71 58 ) ) PUNCT eurjchem-20 72 1 , , PUNCT eurjchem-20 72 2     SPACE eurjchem-20 72 3 7.32 7.32 NUM eurjchem-20 72 4     SPACE eurjchem-20 72 5 ( ( PUNCT eurjchem-20 72 6 d d PROPN eurjchem-20 72 7 , , PUNCT eurjchem-20 72 8     SPACE eurjchem-20 72 9 2h 2h NUM eurjchem-20 72 10 , , PUNCT eurjchem-20 72 11     SPACE eurjchem-20 72 12 j=9 j=9 NOUN eurjchem-20 72 13     SPACE eurjchem-20 72 14 hz hz VERB eurjchem-20 72 15 , , PUNCT eurjchem-20 72 16     SPACE eurjchem-20 72 17 ar‐h ar‐h NOUN eurjchem-20 72 18 ) ) PUNCT eurjchem-20 72 19 , , PUNCT eurjchem-20 72 20     SPACE eurjchem-20 72 21 6.8‐6.81 6.8‐6.81 NUM eurjchem-20 72 22     SPACE eurjchem-20 72 23 ( ( PUNCT eurjchem-20 72 24 m m PROPN eurjchem-20 72 25 , , PUNCT eurjchem-20 72 26     SPACE eurjchem-20 72 27 1h 1h NUM eurjchem-20 72 28 , , PUNCT eurjchem-20 72 29     SPACE eurjchem-20 72 30 h‐1 h‐1 PROPN eurjchem-20 72 31 ' ' PUNCT eurjchem-20 72 32 ) ) PUNCT eurjchem-20 72 33 , , PUNCT eurjchem-20 72 34     SPACE eurjchem-20 72 35 6.32‐ 6.32‐ NUM eurjchem-20 72 36 6.34 6.34 NUM eurjchem-20 72 37     SPACE eurjchem-20 72 38 ( ( PUNCT eurjchem-20 72 39 m m PROPN eurjchem-20 72 40 , , PUNCT eurjchem-20 72 41     SPACE eurjchem-20 72 42 1h 1h NUM eurjchem-20 72 43 , , PUNCT eurjchem-20 72 44     SPACE eurjchem-20 72 45 h‐2 h‐2 NOUN eurjchem-20 72 46 ' ' PUNCT eurjchem-20 72 47 ) ) PUNCT eurjchem-20 72 48 , , PUNCT eurjchem-20 72 49     SPACE eurjchem-20 72 50 5.89‐5.90 5.89‐5.90 NUM eurjchem-20 72 51     SPACE eurjchem-20 72 52 ( ( PUNCT eurjchem-20 72 53 m m PROPN eurjchem-20 72 54 , , PUNCT eurjchem-20 72 55     SPACE eurjchem-20 72 56 1h 1h NUM eurjchem-20 72 57 , , PUNCT eurjchem-20 72 58     SPACE eurjchem-20 72 59 h‐3 h‐3 NOUN eurjchem-20 72 60 ' ' PUNCT eurjchem-20 72 61 ) ) PUNCT eurjchem-20 72 62 , , PUNCT eurjchem-20 72 63     SPACE eurjchem-20 72 64 4.8 4.8 NUM eurjchem-20 72 65     SPACE eurjchem-20 72 66 ( ( PUNCT eurjchem-20 72 67 brs br VERB eurjchem-20 72 68 , , PUNCT eurjchem-20 72 69     SPACE eurjchem-20 72 70 1h 1h NUM eurjchem-20 72 71 , , PUNCT eurjchem-20 72 72     SPACE eurjchem-20 72 73 val‐ val‐ PROPN eurjchem-20 72 74 nh nh PROPN eurjchem-20 72 75 ) ) PUNCT eurjchem-20 72 76 , , PUNCT eurjchem-20 72 77     SPACE eurjchem-20 72 78 3.94‐4.00 3.94‐4.00 NUM eurjchem-20 72 79     SPACE eurjchem-20 72 80 ( ( PUNCT eurjchem-20 72 81 m m PROPN eurjchem-20 72 82 , , PUNCT eurjchem-20 72 83     SPACE eurjchem-20 72 84 4h 4h NOUN eurjchem-20 72 85 , , PUNCT eurjchem-20 72 86     SPACE eurjchem-20 72 87 2h‐5 2h‐5 NUM eurjchem-20 72 88 ' ' PUNCT eurjchem-20 72 89 , , PUNCT eurjchem-20 72 90     SPACE eurjchem-20 72 91 h‐4 h‐4 NOUN eurjchem-20 72 92 ' ' PUNCT eurjchem-20 72 93 , , PUNCT eurjchem-20 72 94     SPACE eurjchem-20 72 95 val‐nh‐ch val‐nh‐ch NOUN eurjchem-20 72 96 ) ) PUNCT eurjchem-20 72 97 , , PUNCT eurjchem-20 72 98     SPACE eurjchem-20 72 99 3.01 3.01 NUM eurjchem-20 72 100     SPACE eurjchem-20 72 101 ( ( PUNCT eurjchem-20 72 102 s s PROPN eurjchem-20 72 103 , , PUNCT eurjchem-20 72 104     SPACE eurjchem-20 72 105 3h 3h NUM eurjchem-20 72 106 , , PUNCT eurjchem-20 72 107     SPACE eurjchem-20 72 108 ‐ ‐ NOUN eurjchem-20 72 109 och3 och3 ADJ eurjchem-20 72 110 ) ) PUNCT eurjchem-20 72 111 , , PUNCT eurjchem-20 72 112     SPACE eurjchem-20 72 113 2.51‐2.52 2.51‐2.52 NOUN eurjchem-20 72 114     SPACE eurjchem-20 72 115 ( ( PUNCT eurjchem-20 72 116 m m PROPN eurjchem-20 72 117 , , PUNCT eurjchem-20 72 118     SPACE eurjchem-20 72 119 1h 1h NUM eurjchem-20 72 120 , , PUNCT eurjchem-20 72 121     SPACE eurjchem-20 72 122 ( ( PUNCT eurjchem-20 72 123 ch3)2ch ch3)2ch NOUN eurjchem-20 72 124 ) ) PUNCT eurjchem-20 72 125 , , PUNCT eurjchem-20 72 126     SPACE eurjchem-20 72 127 1.71 1.71 NUM eurjchem-20 72 128     SPACE eurjchem-20 72 129 ( ( PUNCT eurjchem-20 72 130 s s PROPN eurjchem-20 72 131 , , PUNCT eurjchem-20 72 132     SPACE eurjchem-20 72 133 3h 3h NUM eurjchem-20 72 134 , , PUNCT eurjchem-20 72 135     SPACE eurjchem-20 72 136 ch3 ch3 PROPN eurjchem-20 72 137 ) ) PUNCT eurjchem-20 72 138 , , PUNCT eurjchem-20 72 139     SPACE eurjchem-20 72 140 1.15‐1.18 1.15‐1.18 NUM eurjchem-20 72 141     SPACE eurjchem-20 72 142 ( ( PUNCT eurjchem-20 72 143 d d PROPN eurjchem-20 72 144 , , PUNCT eurjchem-20 72 145     SPACE eurjchem-20 72 146 6h 6h NOUN eurjchem-20 72 147 , , PUNCT eurjchem-20 72 148     SPACE eurjchem-20 72 149 ( ( PUNCT eurjchem-20 72 150 ch3)2c‐ ch3)2c‐ PROPN eurjchem-20 72 151 ) ) PUNCT eurjchem-20 72 152 . . PUNCT eurjchem-20 72 153     SPACE eurjchem-20 73 1 13c‐nmr 13c‐nmr NOUN eurjchem-20 73 2     SPACE eurjchem-20 73 3 ( ( PUNCT eurjchem-20 73 4 125 125 NUM eurjchem-20 73 5     SPACE eurjchem-20 73 6 mhz mhz NOUN eurjchem-20 73 7 , , PUNCT eurjchem-20 73 8     SPACE eurjchem-20 73 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 73 10 , , PUNCT eurjchem-20 73 11     SPACE eurjchem-20 73 12   NUM eurjchem-20 73 13 ): ): PUNCT eurjchem-20 73 14     SPACE eurjchem-20 73 15 172.5 172.5 NUM eurjchem-20 73 16     SPACE eurjchem-20 73 17 ( ( PUNCT eurjchem-20 73 18 val‐ val‐ ADP eurjchem-20 73 19 c c PROPN eurjchem-20 73 20 = = NOUN eurjchem-20 73 21 o o NOUN eurjchem-20 73 22 ) ) PUNCT eurjchem-20 73 23 , , PUNCT eurjchem-20 73 24     SPACE eurjchem-20 73 25 164.39 164.39 NUM eurjchem-20 73 26     SPACE eurjchem-20 73 27 ( ( PUNCT eurjchem-20 73 28 c‐4 c‐4 PROPN eurjchem-20 73 29 ) ) PUNCT eurjchem-20 73 30 , , PUNCT eurjchem-20 73 31     SPACE eurjchem-20 73 32 159.8 159.8 NUM eurjchem-20 73 33     SPACE eurjchem-20 73 34 ( ( PUNCT eurjchem-20 73 35 c‐2),151.2 c‐2),151.2 NOUN eurjchem-20 73 36     SPACE eurjchem-20 73 37 ( ( PUNCT eurjchem-20 73 38 c‐1 c‐1 NOUN eurjchem-20 73 39 '' '' PUNCT eurjchem-20 73 40 ) ) PUNCT eurjchem-20 73 41 , , PUNCT eurjchem-20 73 42     SPACE eurjchem-20 73 43 142.3 142.3 NUM eurjchem-20 73 44     SPACE eurjchem-20 73 45 ( ( PUNCT eurjchem-20 73 46 c‐4 c‐4 PROPN eurjchem-20 73 47 '' '' PUNCT eurjchem-20 73 48 ) ) PUNCT eurjchem-20 73 49 , , PUNCT eurjchem-20 73 50     SPACE eurjchem-20 73 51 137 137 NUM eurjchem-20 73 52     SPACE eurjchem-20 73 53 ( ( PUNCT eurjchem-20 73 54 c‐6 c‐6 NOUN eurjchem-20 73 55 ) ) PUNCT eurjchem-20 73 56 , , PUNCT eurjchem-20 73 57     SPACE eurjchem-20 73 58 134.5 134.5 NUM eurjchem-20 73 59     SPACE eurjchem-20 73 60 ( ( PUNCT eurjchem-20 73 61 c‐3 c‐3 NOUN eurjchem-20 73 62 ' ' PUNCT eurjchem-20 73 63 ) ) PUNCT eurjchem-20 73 64 , , PUNCT eurjchem-20 73 65     SPACE eurjchem-20 73 66 126.7 126.7 NUM eurjchem-20 73 67     SPACE eurjchem-20 73 68 ( ( PUNCT eurjchem-20 73 69 c‐3 c‐3 NOUN eurjchem-20 73 70 '' '' PUNCT eurjchem-20 73 71 , , PUNCT eurjchem-20 73 72     SPACE eurjchem-20 73 73 c‐5 c‐5 NOUN eurjchem-20 73 74 '' '' PUNCT eurjchem-20 73 75 ) ) PUNCT eurjchem-20 73 76 , , PUNCT eurjchem-20 73 77     SPACE eurjchem-20 73 78 125.4 125.4 NUM eurjchem-20 73 79     SPACE eurjchem-20 73 80 ( ( PUNCT eurjchem-20 73 81 c‐2 c‐2 NOUN eurjchem-20 73 82 ' ' PUNCT eurjchem-20 73 83 ) ) PUNCT eurjchem-20 73 84 , , PUNCT eurjchem-20 73 85     SPACE eurjchem-20 73 86 120.7 120.7 NUM eurjchem-20 73 87     SPACE eurjchem-20 73 88 ( ( PUNCT eurjchem-20 73 89 c‐2 c‐2 NOUN eurjchem-20 73 90 '' '' PUNCT eurjchem-20 73 91 , , PUNCT eurjchem-20 73 92     SPACE eurjchem-20 73 93 c‐6 c‐6 NOUN eurjchem-20 73 94 '' '' PUNCT eurjchem-20 73 95 ) ) PUNCT eurjchem-20 73 96 , , PUNCT eurjchem-20 73 97     SPACE eurjchem-20 73 98 110.9 110.9 NUM eurjchem-20 73 99     SPACE eurjchem-20 73 100 ( ( PUNCT eurjchem-20 73 101 c‐5 c‐5 NOUN eurjchem-20 73 102 ) ) PUNCT eurjchem-20 73 103 , , PUNCT eurjchem-20 73 104     SPACE eurjchem-20 73 105 89.2 89.2 NUM eurjchem-20 73 106     SPACE eurjchem-20 73 107 ( ( PUNCT eurjchem-20 73 108 c‐1 c‐1 NOUN eurjchem-20 73 109 ' ' PUNCT eurjchem-20 73 110 ) ) PUNCT eurjchem-20 73 111 , , PUNCT eurjchem-20 73 112     SPACE eurjchem-20 73 113 85.7 85.7 NUM eurjchem-20 73 114     SPACE eurjchem-20 73 115 ( ( PUNCT eurjchem-20 73 116 c‐4 c‐4 PROPN eurjchem-20 73 117 ' ' PUNCT eurjchem-20 73 118 ) ) PUNCT eurjchem-20 73 119 , , PUNCT eurjchem-20 73 120     SPACE eurjchem-20 73 121 66.4 66.4 NUM eurjchem-20 73 122     SPACE eurjchem-20 73 123 ( ( PUNCT eurjchem-20 73 124 c‐5 c‐5 NOUN eurjchem-20 73 125 ' ' PUNCT eurjchem-20 73 126 ) ) PUNCT eurjchem-20 73 127 , , PUNCT eurjchem-20 73 128     SPACE eurjchem-20 73 129 46 46 NUM eurjchem-20 73 130     SPACE eurjchem-20 73 131 ( ( PUNCT eurjchem-20 73 132 val‐ val‐ PROPN eurjchem-20 73 133 ch ch NOUN eurjchem-20 73 134 ) ) PUNCT eurjchem-20 73 135 , , PUNCT eurjchem-20 73 136     SPACE eurjchem-20 73 137 43.1(‐och3 43.1(‐och3 NOUN eurjchem-20 73 138 ) ) PUNCT eurjchem-20 73 139 , , PUNCT eurjchem-20 73 140     SPACE eurjchem-20 73 141 33.2 33.2 NUM eurjchem-20 73 142     SPACE eurjchem-20 73 143 ( ( PUNCT eurjchem-20 73 144 ch3)2c‐ ch3)2c‐ PROPN eurjchem-20 73 145 ) ) PUNCT eurjchem-20 73 146 , , PUNCT eurjchem-20 73 147     SPACE eurjchem-20 73 148 18.9 18.9 NUM eurjchem-20 73 149     SPACE eurjchem-20 73 150 ( ( PUNCT eurjchem-20 73 151 ch3)2c‐ ch3)2c‐ PROPN eurjchem-20 73 152 ) ) PUNCT eurjchem-20 73 153 , , PUNCT eurjchem-20 73 154     SPACE eurjchem-20 73 155 12.2 12.2 NUM eurjchem-20 73 156     SPACE eurjchem-20 73 157 ( ( PUNCT eurjchem-20 73 158 ‐ch3 ‐ch3 ADJ eurjchem-20 73 159 ) ) PUNCT eurjchem-20 73 160 . . PUNCT eurjchem-20 73 161     SPACE eurjchem-20 74 1 31p‐nmr 31p‐nmr NOUN eurjchem-20 74 2     SPACE eurjchem-20 74 3 ( ( PUNCT eurjchem-20 74 4 202 202 NUM eurjchem-20 74 5     SPACE eurjchem-20 74 6 mhz mhz NOUN eurjchem-20 74 7 , , PUNCT eurjchem-20 74 8     SPACE eurjchem-20 74 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 74 10 , , PUNCT eurjchem-20 74 11     SPACE eurjchem-20 74 12   NUM eurjchem-20 74 13 ): ): PUNCT eurjchem-20 74 14     SPACE eurjchem-20 74 15 2.85 2.85 NUM eurjchem-20 74 16 . . PUNCT eurjchem-20 74 17     SPACE eurjchem-20 74 18 gcms gcms PROPN eurjchem-20 74 19     SPACE eurjchem-20 74 20 ( ( PUNCT eurjchem-20 74 21 m m PROPN eurjchem-20 74 22 / / SYM eurjchem-20 74 23 z z NOUN eurjchem-20 74 24 ; ; PUNCT eurjchem-20 74 25     SPACE eurjchem-20 74 26 % % NOUN eurjchem-20 74 27 ): ): PUNCT eurjchem-20 74 28     SPACE eurjchem-20 74 29 ( ( PUNCT eurjchem-20 74 30 539.25 539.25 NUM eurjchem-20 74 31 , , PUNCT eurjchem-20 74 32     SPACE eurjchem-20 74 33 27 27 NUM eurjchem-20 74 34 % % NOUN eurjchem-20 74 35 ) ) PUNCT eurjchem-20 74 36     SPACE eurjchem-20 75 1 [ [ X eurjchem-20 75 2 mh]+ mh]+ X eurjchem-20 75 3 . . PUNCT eurjchem-20 75 4           SPACE eurjchem-20 75 5 2.2.9 2.2.9 NUM eurjchem-20 75 6 . . PUNCT eurjchem-20 75 7     SPACE eurjchem-20 75 8 ( ( PUNCT eurjchem-20 75 9 2s)­methyl 2s)­methyl PROPN eurjchem-20 75 10     SPACE eurjchem-20 75 11 4­methyl­2­((s)­((5­(5­methyl­2 4­methyl­2­((s)­((5­(5­methyl­2 NUM eurjchem-20 75 12 , , PUNCT eurjchem-20 75 13     SPACE eurjchem-20 75 14 4­dioxo­ 4­dioxo­ NUM eurjchem-20 75 15 3,4­dihydropyrimidin­1(2h)­yl)­2,5­dihydrofuran­2­yl)meth 3,4­dihydropyrimidin­1(2h)­yl)­2,5­dihydrofuran­2­yl)meth NUM eurjchem-20 75 16     SPACE eurjchem-20 75 17 oxy)(4­nitrophenoxy)phosphorylamino)pentanoate oxy)(4­nitrophenoxy)phosphorylamino)pentanoate ADJ eurjchem-20 75 18     SPACE eurjchem-20 75 19 ( ( PUNCT eurjchem-20 75 20 4i 4i NUM eurjchem-20 75 21 ) ) PUNCT eurjchem-20 75 22         SPACE eurjchem-20 75 23 yield yield NOUN eurjchem-20 75 24 : : PUNCT eurjchem-20 75 25     SPACE eurjchem-20 75 26 63 63 NUM eurjchem-20 75 27 % % NOUN eurjchem-20 75 28 . . PUNCT eurjchem-20 75 29     SPACE eurjchem-20 76 1 m.p m.p PROPN eurjchem-20 76 2 . . PROPN eurjchem-20 76 3 : : PUNCT eurjchem-20 76 4     SPACE eurjchem-20 76 5 151‐153 151‐153 NUM eurjchem-20 76 6     SPACE eurjchem-20 76 7 oc oc PROPN eurjchem-20 76 8     SPACE eurjchem-20 76 9 . . PUNCT eurjchem-20 76 10     SPACE eurjchem-20 77 1 ir ir VERB eurjchem-20 77 2     SPACE eurjchem-20 77 3 ( ( PUNCT eurjchem-20 77 4 kbr kbr PROPN eurjchem-20 77 5 , , PUNCT eurjchem-20 77 6     SPACE eurjchem-20 77 7 cm‐1 cm‐1 NOUN eurjchem-20 77 8 ): ): PUNCT eurjchem-20 77 9     SPACE eurjchem-20 77 10 3387 3387 NUM eurjchem-20 77 11     SPACE eurjchem-20 77 12 ν(‐nh ν(‐nh PROPN eurjchem-20 77 13 ) ) PUNCT eurjchem-20 77 14 , , PUNCT eurjchem-20 77 15     SPACE eurjchem-20 77 16 1675 1675 NUM eurjchem-20 77 17 , , PUNCT eurjchem-20 77 18     SPACE eurjchem-20 77 19 1728 1728 NUM eurjchem-20 77 20     SPACE eurjchem-20 77 21 ν(c ν(c PROPN eurjchem-20 77 22 = = NOUN eurjchem-20 77 23 o o NOUN eurjchem-20 77 24 ) ) PUNCT eurjchem-20 77 25 , , PUNCT eurjchem-20 77 26     SPACE eurjchem-20 77 27 1232 1232 NUM eurjchem-20 77 28     SPACE eurjchem-20 77 29 ν(p ν(p NOUN eurjchem-20 77 30 = = SYM eurjchem-20 77 31 o o NOUN eurjchem-20 77 32 ) ) PUNCT eurjchem-20 77 33 . . PUNCT eurjchem-20 77 34     SPACE eurjchem-20 78 1 1h‐nmr 1h‐nmr NUM eurjchem-20 78 2     SPACE eurjchem-20 78 3 ( ( PUNCT eurjchem-20 78 4 500 500 NUM eurjchem-20 78 5     SPACE eurjchem-20 78 6 mhz mhz NOUN eurjchem-20 78 7 , , PUNCT eurjchem-20 78 8     SPACE eurjchem-20 78 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 78 10 , , PUNCT eurjchem-20 78 11     SPACE eurjchem-20 78 12   NUM eurjchem-20 78 13 ): ): PUNCT eurjchem-20 78 14     SPACE eurjchem-20 78 15 8.7 8.7 NUM eurjchem-20 78 16     SPACE eurjchem-20 78 17 ( ( PUNCT eurjchem-20 78 18 s s PROPN eurjchem-20 78 19 , , PUNCT eurjchem-20 78 20     SPACE eurjchem-20 78 21 1h 1h NUM eurjchem-20 78 22 , , PUNCT eurjchem-20 78 23     SPACE eurjchem-20 78 24 nh nh PROPN eurjchem-20 78 25 ) ) PUNCT eurjchem-20 78 26 , , PUNCT eurjchem-20 78 27     SPACE eurjchem-20 78 28 8.21 8.21 NUM eurjchem-20 78 29     SPACE eurjchem-20 78 30 ( ( PUNCT eurjchem-20 78 31 d d PROPN eurjchem-20 78 32 , , PUNCT eurjchem-20 78 33     SPACE eurjchem-20 78 34 2h 2h NUM eurjchem-20 78 35 , , PUNCT eurjchem-20 78 36     SPACE eurjchem-20 78 37 j=7 j=7 NOUN eurjchem-20 78 38     SPACE eurjchem-20 78 39 hz hz VERB eurjchem-20 78 40 , , PUNCT eurjchem-20 78 41     SPACE eurjchem-20 78 42 ar‐h ar‐h NOUN eurjchem-20 78 43 ) ) PUNCT eurjchem-20 78 44 , , PUNCT eurjchem-20 78 45     SPACE eurjchem-20 78 46 7.6 7.6 NUM eurjchem-20 78 47     SPACE eurjchem-20 78 48 ( ( PUNCT eurjchem-20 78 49 d d PROPN eurjchem-20 78 50 , , PUNCT eurjchem-20 78 51     SPACE eurjchem-20 78 52 1h 1h NUM eurjchem-20 78 53 , , PUNCT eurjchem-20 78 54     SPACE eurjchem-20 78 55 j=1 j=1 NOUN eurjchem-20 78 56     SPACE eurjchem-20 78 57 hz hz VERB eurjchem-20 78 58 , , PUNCT eurjchem-20 78 59     SPACE eurjchem-20 78 60 h‐6 h‐6 NOUN eurjchem-20 78 61 ) ) PUNCT eurjchem-20 78 62 , , PUNCT eurjchem-20 78 63     SPACE eurjchem-20 78 64 7.48 7.48 NUM eurjchem-20 78 65     SPACE eurjchem-20 78 66 ( ( PUNCT eurjchem-20 78 67 d d PROPN eurjchem-20 78 68 , , PUNCT eurjchem-20 78 69     SPACE eurjchem-20 78 70 2h 2h NUM eurjchem-20 78 71 , , PUNCT eurjchem-20 78 72     SPACE eurjchem-20 78 73 j=7.5 j=7.5 NOUN eurjchem-20 78 74     SPACE eurjchem-20 78 75 hz hz VERB eurjchem-20 78 76 , , PUNCT eurjchem-20 78 77     SPACE eurjchem-20 78 78 ar‐h ar‐h NOUN eurjchem-20 78 79 ) ) PUNCT eurjchem-20 78 80 , , PUNCT eurjchem-20 78 81     SPACE eurjchem-20 78 82 6.94‐6.95 6.94‐6.95 NOUN eurjchem-20 78 83     SPACE eurjchem-20 78 84 ( ( PUNCT eurjchem-20 78 85 m m PROPN eurjchem-20 78 86 , , PUNCT eurjchem-20 78 87     SPACE eurjchem-20 78 88 1h 1h NUM eurjchem-20 78 89 , , PUNCT eurjchem-20 78 90     SPACE eurjchem-20 78 91 h‐1 h‐1 PROPN eurjchem-20 78 92 ' ' PUNCT eurjchem-20 78 93 ) ) PUNCT eurjchem-20 78 94 , , PUNCT eurjchem-20 78 95     SPACE eurjchem-20 79 1 6.3‐ 6.3‐ NUM eurjchem-20 79 2 6.33 6.33 NUM eurjchem-20 79 3     SPACE eurjchem-20 79 4 ( ( PUNCT eurjchem-20 79 5 m m PROPN eurjchem-20 79 6 , , PUNCT eurjchem-20 79 7     SPACE eurjchem-20 79 8 1h 1h NUM eurjchem-20 79 9 , , PUNCT eurjchem-20 79 10     SPACE eurjchem-20 79 11 h‐2 h‐2 NOUN eurjchem-20 79 12 ' ' PUNCT eurjchem-20 79 13 ) ) PUNCT eurjchem-20 79 14 , , PUNCT eurjchem-20 79 15     SPACE eurjchem-20 79 16 5.89‐5.92 5.89‐5.92 NUM eurjchem-20 79 17     SPACE eurjchem-20 79 18 ( ( PUNCT eurjchem-20 79 19 m m PROPN eurjchem-20 79 20 , , PUNCT eurjchem-20 79 21     SPACE eurjchem-20 79 22 1h 1h NUM eurjchem-20 79 23 , , PUNCT eurjchem-20 79 24     SPACE eurjchem-20 79 25 h‐3 h‐3 NOUN eurjchem-20 79 26 ' ' PUNCT eurjchem-20 79 27 ) ) PUNCT eurjchem-20 79 28 , , PUNCT eurjchem-20 79 29     SPACE eurjchem-20 79 30 5.2 5.2 NUM eurjchem-20 79 31     SPACE eurjchem-20 79 32 ( ( PUNCT eurjchem-20 79 33 brs br VERB eurjchem-20 79 34 , , PUNCT eurjchem-20 79 35     SPACE eurjchem-20 79 36 1h 1h NUM eurjchem-20 79 37 , , PUNCT eurjchem-20 79 38     SPACE eurjchem-20 79 39 leu leu PROPN eurjchem-20 79 40     SPACE eurjchem-20 79 41 ‐ ‐ PROPN eurjchem-20 79 42 nh nh PROPN eurjchem-20 79 43 ) ) PUNCT eurjchem-20 79 44 , , PUNCT eurjchem-20 79 45     SPACE eurjchem-20 79 46 3.32‐3.36 3.32‐3.36 NUM eurjchem-20 79 47     SPACE eurjchem-20 79 48 ( ( PUNCT eurjchem-20 79 49 m m PROPN eurjchem-20 79 50 , , PUNCT eurjchem-20 79 51     SPACE eurjchem-20 79 52 4h 4h NOUN eurjchem-20 79 53 , , PUNCT eurjchem-20 79 54     SPACE eurjchem-20 79 55 2h‐5 2h‐5 NUM eurjchem-20 79 56 ' ' PUNCT eurjchem-20 79 57 , , PUNCT eurjchem-20 79 58     SPACE eurjchem-20 79 59 h‐4 h‐4 NOUN eurjchem-20 79 60 ' ' PART eurjchem-20 79 61 , , PUNCT eurjchem-20 79 62     SPACE eurjchem-20 79 63 leu‐nh‐ch leu‐nh‐ch ADJ eurjchem-20 79 64 ) ) PUNCT eurjchem-20 79 65 , , PUNCT eurjchem-20 79 66     SPACE eurjchem-20 79 67 3.21 3.21 NUM eurjchem-20 79 68     SPACE eurjchem-20 79 69 ( ( PUNCT eurjchem-20 79 70 s s PROPN eurjchem-20 79 71 , , PUNCT eurjchem-20 79 72     SPACE eurjchem-20 79 73 3h 3h NUM eurjchem-20 79 74 , , PUNCT eurjchem-20 79 75     SPACE eurjchem-20 79 76 ‐ ‐ NOUN eurjchem-20 79 77 och3 och3 ADJ eurjchem-20 79 78 ) ) PUNCT eurjchem-20 79 79 , , PUNCT eurjchem-20 79 80     SPACE eurjchem-20 79 81 1.9‐1.93 1.9‐1.93 NUM eurjchem-20 79 82     SPACE eurjchem-20 79 83 ( ( PUNCT eurjchem-20 79 84 m m PROPN eurjchem-20 79 85 , , PUNCT eurjchem-20 79 86     SPACE eurjchem-20 79 87 2h 2h NUM eurjchem-20 79 88 , , PUNCT eurjchem-20 79 89     SPACE eurjchem-20 79 90 leu‐ch2 leu‐ch2 NOUN eurjchem-20 79 91 ) ) PUNCT eurjchem-20 79 92 , , PUNCT eurjchem-20 79 93     SPACE eurjchem-20 79 94 1.51‐1.52 1.51‐1.52 NOUN eurjchem-20 79 95     SPACE eurjchem-20 79 96 ( ( PUNCT eurjchem-20 79 97 m m PROPN eurjchem-20 79 98 , , PUNCT eurjchem-20 79 99     SPACE eurjchem-20 79 100 1h 1h NUM eurjchem-20 79 101 , , PUNCT eurjchem-20 79 102     SPACE eurjchem-20 79 103 ( ( PUNCT eurjchem-20 79 104 ch3)2ch ch3)2ch NOUN eurjchem-20 79 105 ) ) PUNCT eurjchem-20 79 106 , , PUNCT eurjchem-20 79 107     SPACE eurjchem-20 79 108 1.71 1.71 NUM eurjchem-20 79 109     SPACE eurjchem-20 79 110 ( ( PUNCT eurjchem-20 79 111 s s PROPN eurjchem-20 79 112 , , PUNCT eurjchem-20 79 113     SPACE eurjchem-20 79 114 3h 3h NUM eurjchem-20 79 115 , , PUNCT eurjchem-20 79 116     SPACE eurjchem-20 79 117 ch3 ch3 PROPN eurjchem-20 79 118 ) ) PUNCT eurjchem-20 79 119 , , PUNCT eurjchem-20 79 120     SPACE eurjchem-20 79 121 1.17‐1.2 1.17‐1.2 NUM eurjchem-20 79 122     SPACE eurjchem-20 79 123 ( ( PUNCT eurjchem-20 79 124 d d NOUN eurjchem-20 79 125 , , PUNCT eurjchem-20 79 126     SPACE eurjchem-20 79 127 6h 6h NOUN eurjchem-20 79 128 , , PUNCT eurjchem-20 79 129     SPACE eurjchem-20 79 130 ( ( PUNCT eurjchem-20 79 131 ch3)2c‐ ch3)2c‐ PROPN eurjchem-20 79 132 ) ) PUNCT eurjchem-20 79 133 . . PUNCT eurjchem-20 79 134     SPACE eurjchem-20 80 1 31p‐nmr 31p‐nmr NOUN eurjchem-20 80 2     SPACE eurjchem-20 80 3 ( ( PUNCT eurjchem-20 80 4 202 202 NUM eurjchem-20 80 5     SPACE eurjchem-20 80 6 mhz mhz NOUN eurjchem-20 80 7 , , PUNCT eurjchem-20 80 8     SPACE eurjchem-20 80 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 80 10 , , PUNCT eurjchem-20 80 11     SPACE eurjchem-20 80 12   NUM eurjchem-20 80 13 ): ): PUNCT eurjchem-20 80 14     SPACE eurjchem-20 80 15 3.40 3.40 NUM eurjchem-20 80 16 , , PUNCT eurjchem-20 80 17     SPACE eurjchem-20 80 18 4.11 4.11 NUM eurjchem-20 80 19 . . PUNCT eurjchem-20 80 20     SPACE eurjchem-20 80 21 gcms gcms PROPN eurjchem-20 80 22     SPACE eurjchem-20 80 23 ( ( PUNCT eurjchem-20 80 24 m m PROPN eurjchem-20 80 25 / / SYM eurjchem-20 80 26 z z NOUN eurjchem-20 80 27 ; ; PUNCT eurjchem-20 80 28     SPACE eurjchem-20 80 29 % % NOUN eurjchem-20 80 30 ): ): PUNCT eurjchem-20 80 31     SPACE eurjchem-20 80 32 ( ( PUNCT eurjchem-20 80 33 553.35 553.35 NUM eurjchem-20 80 34 , , PUNCT eurjchem-20 80 35     SPACE eurjchem-20 80 36 35 35 NUM eurjchem-20 80 37 % % NOUN eurjchem-20 80 38 ) ) PUNCT eurjchem-20 80 39     SPACE eurjchem-20 81 1 [ [ X eurjchem-20 81 2 mh]+ mh]+ X eurjchem-20 81 3 . . PUNCT eurjchem-20 81 4           SPACE eurjchem-20 81 5 2.2.10 2.2.10 NUM eurjchem-20 81 6 . . PUNCT eurjchem-20 81 7     SPACE eurjchem-20 81 8 ( ( PUNCT eurjchem-20 81 9 2r)­ethyl 2r)­ethyl NUM eurjchem-20 81 10     SPACE eurjchem-20 81 11 2­amino­3­((r)­((5­(5­methyl­2,4­dioxo­ 2­amino­3­((r)­((5­(5­methyl­2,4­dioxo­ NUM eurjchem-20 81 12 3,4­dihydropyrimidin­1(2h)­yl)­2,5­dihydrofuran­2­yl 3,4­dihydropyrimidin­1(2h)­yl)­2,5­dihydrofuran­2­yl NUM eurjchem-20 81 13 ) ) PUNCT eurjchem-20 81 14     SPACE eurjchem-20 81 15 methoxy)(4­nitrophenoxy)phosphorylthio)propanoate methoxy)(4­nitrophenoxy)phosphorylthio)propanoate NOUN eurjchem-20 81 16     SPACE eurjchem-20 81 17 ( ( PUNCT eurjchem-20 81 18 4j 4j NOUN eurjchem-20 81 19 ) ) PUNCT eurjchem-20 81 20         SPACE eurjchem-20 81 21 yield yield NOUN eurjchem-20 81 22 : : PUNCT eurjchem-20 81 23     SPACE eurjchem-20 81 24 59 59 NUM eurjchem-20 81 25 % % NOUN eurjchem-20 81 26 . . PUNCT eurjchem-20 81 27     SPACE eurjchem-20 82 1 m.p m.p PROPN eurjchem-20 82 2 . . PROPN eurjchem-20 82 3 : : PUNCT eurjchem-20 82 4     SPACE eurjchem-20 82 5 138‐141 138‐141 NUM eurjchem-20 82 6     SPACE eurjchem-20 82 7 oc oc NOUN eurjchem-20 82 8 , , PUNCT eurjchem-20 82 9     SPACE eurjchem-20 82 10 anal anal ADJ eurjchem-20 82 11 . . PUNCT eurjchem-20 82 12     SPACE eurjchem-20 82 13 calcd calcd NOUN eurjchem-20 82 14 . . PUNCT eurjchem-20 82 15     SPACE eurjchem-20 82 16 for for ADP eurjchem-20 82 17     SPACE eurjchem-20 82 18 c21h25n4o10ps c21h25n4o10ps PROPN eurjchem-20 82 19 : : PUNCT eurjchem-20 82 20     SPACE eurjchem-20 82 21 c c X eurjchem-20 82 22 , , PUNCT eurjchem-20 82 23     SPACE eurjchem-20 82 24 45.32 45.32 NUM eurjchem-20 82 25 ; ; PUNCT eurjchem-20 82 26     SPACE eurjchem-20 82 27 h h NOUN eurjchem-20 82 28 , , PUNCT eurjchem-20 82 29     SPACE eurjchem-20 82 30 4.53 4.53 NUM eurjchem-20 82 31 ; ; PUNCT eurjchem-20 82 32     SPACE eurjchem-20 82 33 n n CCONJ eurjchem-20 82 34 , , PUNCT eurjchem-20 82 35     SPACE eurjchem-20 82 36 10.07;found 10.07;found NUM eurjchem-20 82 37     SPACE eurjchem-20 82 38 c c NOUN eurjchem-20 82 39 , , PUNCT eurjchem-20 82 40     SPACE eurjchem-20 82 41 45.27 45.27 NUM eurjchem-20 82 42 ; ; PUNCT eurjchem-20 82 43     SPACE eurjchem-20 82 44 h h NOUN eurjchem-20 82 45 , , PUNCT eurjchem-20 82 46     SPACE eurjchem-20 82 47 4.49 4.49 NUM eurjchem-20 82 48 ; ; PUNCT eurjchem-20 82 49     SPACE eurjchem-20 82 50 n n CCONJ eurjchem-20 82 51 , , PUNCT eurjchem-20 82 52     SPACE eurjchem-20 82 53 10.11 10.11 NUM eurjchem-20 82 54 . . PUNCT eurjchem-20 82 55     SPACE eurjchem-20 83 1 ir ir VERB eurjchem-20 83 2     SPACE eurjchem-20 83 3 ( ( PUNCT eurjchem-20 83 4 kbr kbr PROPN eurjchem-20 83 5 , , PUNCT eurjchem-20 83 6     SPACE eurjchem-20 83 7 cm‐1 cm‐1 NOUN eurjchem-20 83 8 ): ): PUNCT eurjchem-20 83 9     SPACE eurjchem-20 83 10 3375 3375 NUM eurjchem-20 83 11     SPACE eurjchem-20 83 12 ν(‐nh ν(‐nh PROPN eurjchem-20 83 13 ) ) PUNCT eurjchem-20 83 14 , , PUNCT eurjchem-20 83 15     SPACE eurjchem-20 83 16 1677 1677 NUM eurjchem-20 83 17 , , PUNCT eurjchem-20 83 18     SPACE eurjchem-20 83 19 1727 1727 NUM eurjchem-20 83 20     SPACE eurjchem-20 83 21 ν(c ν(c PROPN eurjchem-20 83 22 = = NOUN eurjchem-20 83 23 o o NOUN eurjchem-20 83 24 ) ) PUNCT eurjchem-20 83 25 , , PUNCT eurjchem-20 83 26     SPACE eurjchem-20 83 27 1228 1228 NUM eurjchem-20 83 28     SPACE eurjchem-20 83 29 ν(p ν(p PROPN eurjchem-20 83 30 = = SYM eurjchem-20 83 31 o o NOUN eurjchem-20 83 32 ) ) PUNCT eurjchem-20 83 33 . . PUNCT eurjchem-20 83 34     SPACE eurjchem-20 84 1 1h‐nmr 1h‐nmr NUM eurjchem-20 84 2     SPACE eurjchem-20 84 3 ( ( PUNCT eurjchem-20 84 4 500 500 NUM eurjchem-20 84 5     SPACE eurjchem-20 84 6 mhz mhz NOUN eurjchem-20 84 7 , , PUNCT eurjchem-20 84 8     SPACE eurjchem-20 84 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 84 10 , , PUNCT eurjchem-20 84 11     SPACE eurjchem-20 84 12   NUM eurjchem-20 84 13 ): ): PUNCT eurjchem-20 84 14     SPACE eurjchem-20 84 15 9.4 9.4 NUM eurjchem-20 84 16     SPACE eurjchem-20 84 17 ( ( PUNCT eurjchem-20 84 18 s s PROPN eurjchem-20 84 19 , , PUNCT eurjchem-20 84 20     SPACE eurjchem-20 84 21 1h 1h NUM eurjchem-20 84 22 , , PUNCT eurjchem-20 84 23     SPACE eurjchem-20 84 24 nh nh PROPN eurjchem-20 84 25 ) ) PUNCT eurjchem-20 84 26 , , PUNCT eurjchem-20 84 27     SPACE eurjchem-20 84 28 8.21 8.21 NUM eurjchem-20 84 29     SPACE eurjchem-20 84 30 ( ( PUNCT eurjchem-20 84 31 d d PROPN eurjchem-20 84 32 , , PUNCT eurjchem-20 84 33     SPACE eurjchem-20 84 34 2h 2h NUM eurjchem-20 84 35 , , PUNCT eurjchem-20 84 36     SPACE eurjchem-20 84 37 j=9.5 j=9.5 NOUN eurjchem-20 84 38     SPACE eurjchem-20 84 39 hz hz VERB eurjchem-20 84 40 , , PUNCT eurjchem-20 84 41     SPACE eurjchem-20 84 42 ar‐h ar‐h NOUN eurjchem-20 84 43 ) ) PUNCT eurjchem-20 84 44 , , PUNCT eurjchem-20 84 45     SPACE eurjchem-20 84 46 8.11(d 8.11(d NOUN eurjchem-20 84 47 , , PUNCT eurjchem-20 84 48     SPACE eurjchem-20 84 49 2h 2h NUM eurjchem-20 84 50 , , PUNCT eurjchem-20 84 51     SPACE eurjchem-20 85 1 j=9 j=9 NOUN eurjchem-20 85 2     SPACE eurjchem-20 85 3 hz hz VERB eurjchem-20 85 4 , , PUNCT eurjchem-20 85 5     SPACE eurjchem-20 85 6 ar‐h ar‐h NOUN eurjchem-20 85 7 ) ) PUNCT eurjchem-20 85 8 , , PUNCT eurjchem-20 85 9     SPACE eurjchem-20 85 10 7.43 7.43 NUM eurjchem-20 85 11     SPACE eurjchem-20 85 12 ( ( PUNCT eurjchem-20 85 13 d d PROPN eurjchem-20 85 14 , , PUNCT eurjchem-20 85 15     SPACE eurjchem-20 85 16 1h 1h NUM eurjchem-20 85 17 , , PUNCT eurjchem-20 85 18     SPACE eurjchem-20 85 19 j=1 j=1 NOUN eurjchem-20 85 20     SPACE eurjchem-20 85 21 hz hz VERB eurjchem-20 85 22 , , PUNCT eurjchem-20 85 23     SPACE eurjchem-20 85 24 h‐6 h‐6 NOUN eurjchem-20 85 25 ) ) PUNCT eurjchem-20 85 26 , , PUNCT eurjchem-20 85 27     SPACE eurjchem-20 86 1 6.95‐6.97 6.95‐6.97 NOUN eurjchem-20 86 2     SPACE eurjchem-20 86 3 ( ( PUNCT eurjchem-20 86 4 m m PROPN eurjchem-20 86 5 , , PUNCT eurjchem-20 86 6     SPACE eurjchem-20 86 7 1h 1h NUM eurjchem-20 86 8 , , PUNCT eurjchem-20 86 9     SPACE eurjchem-20 86 10 h‐1 h‐1 PROPN eurjchem-20 86 11 ' ' PUNCT eurjchem-20 86 12 ) ) PUNCT eurjchem-20 86 13 , , PUNCT eurjchem-20 86 14     SPACE eurjchem-20 86 15 6.29‐6.31 6.29‐6.31 NUM eurjchem-20 86 16     SPACE eurjchem-20 86 17 ( ( PUNCT eurjchem-20 86 18 m m PROPN eurjchem-20 86 19 , , PUNCT eurjchem-20 86 20     SPACE eurjchem-20 86 21 1h 1h NUM eurjchem-20 86 22 , , PUNCT eurjchem-20 86 23     SPACE eurjchem-20 86 24 h‐ h‐ PROPN eurjchem-20 86 25 2 2 NUM eurjchem-20 86 26 ' ' NUM eurjchem-20 86 27 ) ) PUNCT eurjchem-20 86 28 , , PUNCT eurjchem-20 86 29     SPACE eurjchem-20 86 30 5.91‐5.93 5.91‐5.93 NUM eurjchem-20 86 31     SPACE eurjchem-20 86 32 ( ( PUNCT eurjchem-20 86 33 m m PROPN eurjchem-20 86 34 , , PUNCT eurjchem-20 86 35     SPACE eurjchem-20 86 36 1h 1h NUM eurjchem-20 86 37 , , PUNCT eurjchem-20 86 38     SPACE eurjchem-20 86 39 h‐3 h‐3 NOUN eurjchem-20 86 40 ' ' PUNCT eurjchem-20 86 41 ) ) PUNCT eurjchem-20 86 42 , , PUNCT eurjchem-20 86 43     SPACE eurjchem-20 86 44 5.54 5.54 NUM eurjchem-20 86 45     SPACE eurjchem-20 86 46 ( ( PUNCT eurjchem-20 86 47 bs bs PROPN eurjchem-20 86 48 , , PUNCT eurjchem-20 86 49     SPACE eurjchem-20 86 50 2h 2h NUM eurjchem-20 86 51 , , PUNCT eurjchem-20 86 52     SPACE eurjchem-20 86 53 ‐nh2 ‐nh2 NOUN eurjchem-20 86 54 , , PUNCT eurjchem-20 86 55     SPACE eurjchem-20 86 56 ) ) PUNCT eurjchem-20 86 57 , , PUNCT eurjchem-20 86 58     SPACE eurjchem-20 86 59 3.92‐3.98 3.92‐3.98 NUM eurjchem-20 86 60     SPACE eurjchem-20 86 61 ( ( PUNCT eurjchem-20 86 62 m m PROPN eurjchem-20 86 63 , , PUNCT eurjchem-20 86 64     SPACE eurjchem-20 86 65 4h 4h NOUN eurjchem-20 86 66 , , PUNCT eurjchem-20 86 67     SPACE eurjchem-20 86 68 2h‐5 2h‐5 NOUN eurjchem-20 86 69 ' ' PUNCT eurjchem-20 86 70 , , PUNCT eurjchem-20 86 71     SPACE eurjchem-20 86 72 h‐4 h‐4 NOUN eurjchem-20 86 73 ' ' PUNCT eurjchem-20 86 74 , , PUNCT eurjchem-20 86 75     SPACE eurjchem-20 86 76 cys‐ch‐ cys‐ch‐ NOUN eurjchem-20 86 77     SPACE eurjchem-20 86 78 nh2 nh2 PROPN eurjchem-20 86 79 ) ) PUNCT eurjchem-20 86 80 , , PUNCT eurjchem-20 86 81     SPACE eurjchem-20 86 82 3.65 3.65 NUM eurjchem-20 86 83     SPACE eurjchem-20 86 84 ( ( PUNCT eurjchem-20 86 85 q q NOUN eurjchem-20 86 86 , , PUNCT eurjchem-20 86 87     SPACE eurjchem-20 86 88 2h 2h NUM eurjchem-20 86 89 , , PUNCT eurjchem-20 86 90     SPACE eurjchem-20 86 91 ‐o‐ch2‐ch3 ‐o‐ch2‐ch3 ADJ eurjchem-20 86 92 ) ) PUNCT eurjchem-20 86 93 , , PUNCT eurjchem-20 86 94     SPACE eurjchem-20 86 95 2.97 2.97 NUM eurjchem-20 86 96     SPACE eurjchem-20 86 97 ‐ ‐ ADV eurjchem-20 86 98 3.05 3.05 NUM eurjchem-20 86 99     SPACE eurjchem-20 86 100 ( ( PUNCT eurjchem-20 86 101 m m PROPN eurjchem-20 86 102 , , PUNCT eurjchem-20 86 103     SPACE eurjchem-20 86 104 2h 2h NUM eurjchem-20 86 105 , , PUNCT eurjchem-20 86 106     SPACE eurjchem-20 86 107 cys cys NOUN eurjchem-20 86 108     SPACE eurjchem-20 86 109 ‐ch2 ‐ch2 NUM eurjchem-20 86 110 ) ) PUNCT eurjchem-20 86 111 , , PUNCT eurjchem-20 86 112     SPACE eurjchem-20 86 113 1.73 1.73 NUM eurjchem-20 86 114     SPACE eurjchem-20 86 115 ( ( PUNCT eurjchem-20 86 116 s s PROPN eurjchem-20 86 117 , , PUNCT eurjchem-20 86 118     SPACE eurjchem-20 86 119 3h 3h NUM eurjchem-20 86 120 , , PUNCT eurjchem-20 86 121     SPACE eurjchem-20 86 122 ch3 ch3 PROPN eurjchem-20 86 123 ) ) PUNCT eurjchem-20 86 124 . . PUNCT eurjchem-20 86 125     SPACE eurjchem-20 87 1 13c‐nmr 13c‐nmr NOUN eurjchem-20 87 2     SPACE eurjchem-20 87 3 ( ( PUNCT eurjchem-20 87 4 125 125 NUM eurjchem-20 87 5     SPACE eurjchem-20 87 6 mhz mhz NOUN eurjchem-20 87 7 , , PUNCT eurjchem-20 87 8     SPACE eurjchem-20 87 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 87 10 , , PUNCT eurjchem-20 87 11     SPACE eurjchem-20 87 12   NUM eurjchem-20 87 13 ): ): PUNCT eurjchem-20 87 14     SPACE eurjchem-20 87 15 172.6 172.6 NUM eurjchem-20 87 16     SPACE eurjchem-20 87 17 ( ( PUNCT eurjchem-20 87 18 cys‐c cys‐c PROPN eurjchem-20 87 19 = = SYM eurjchem-20 87 20 o o NOUN eurjchem-20 87 21 ) ) PUNCT eurjchem-20 87 22 , , PUNCT eurjchem-20 87 23     SPACE eurjchem-20 87 24 159.1 159.1 NUM eurjchem-20 87 25     SPACE eurjchem-20 87 26 ( ( PUNCT eurjchem-20 87 27 c‐4 c‐4 PROPN eurjchem-20 87 28 ) ) PUNCT eurjchem-20 87 29 , , PUNCT eurjchem-20 87 30     SPACE eurjchem-20 87 31 158.1 158.1 NUM eurjchem-20 87 32     SPACE eurjchem-20 87 33 ( ( PUNCT eurjchem-20 87 34 c‐2 c‐2 NOUN eurjchem-20 87 35 ) ) PUNCT eurjchem-20 87 36 , , PUNCT eurjchem-20 87 37     SPACE eurjchem-20 87 38 143.2 143.2 NUM eurjchem-20 87 39     SPACE eurjchem-20 87 40 ( ( PUNCT eurjchem-20 87 41 c‐1 c‐1 NOUN eurjchem-20 87 42 '' '' PUNCT eurjchem-20 87 43 ) ) PUNCT eurjchem-20 87 44 , , PUNCT eurjchem-20 87 45     SPACE eurjchem-20 87 46 142.6 142.6 NUM eurjchem-20 87 47     SPACE eurjchem-20 87 48 ( ( PUNCT eurjchem-20 87 49 c‐4 c‐4 PROPN eurjchem-20 87 50 '' '' PUNCT eurjchem-20 87 51 ) ) PUNCT eurjchem-20 87 52 , , PUNCT eurjchem-20 87 53     SPACE eurjchem-20 87 54 137.5 137.5 NUM eurjchem-20 87 55     SPACE eurjchem-20 87 56 ( ( PUNCT eurjchem-20 87 57 c‐6 c‐6 NOUN eurjchem-20 87 58 ) ) PUNCT eurjchem-20 87 59 , , PUNCT eurjchem-20 87 60     SPACE eurjchem-20 87 61 135.1 135.1 NUM eurjchem-20 87 62     SPACE eurjchem-20 87 63 ( ( PUNCT eurjchem-20 87 64 c‐3 c‐3 NOUN eurjchem-20 87 65 ' ' PUNCT eurjchem-20 87 66 ) ) PUNCT eurjchem-20 87 67 , , PUNCT eurjchem-20 87 68     SPACE eurjchem-20 87 69 125 125 NUM eurjchem-20 87 70     SPACE eurjchem-20 87 71 ( ( PUNCT eurjchem-20 87 72 c‐3 c‐3 NOUN eurjchem-20 87 73 '' '' PUNCT eurjchem-20 87 74 , , PUNCT eurjchem-20 87 75     SPACE eurjchem-20 87 76 c‐5 c‐5 NOUN eurjchem-20 87 77 '' '' PUNCT eurjchem-20 87 78 ) ) PUNCT eurjchem-20 87 79 , , PUNCT eurjchem-20 87 80     SPACE eurjchem-20 87 81 124 124 NUM eurjchem-20 87 82     SPACE eurjchem-20 87 83 ( ( PUNCT eurjchem-20 87 84 c‐2 c‐2 NOUN eurjchem-20 87 85 ' ' PUNCT eurjchem-20 87 86 ) ) PUNCT eurjchem-20 87 87 , , PUNCT eurjchem-20 87 88     SPACE eurjchem-20 87 89 120.5 120.5 NUM eurjchem-20 87 90     SPACE eurjchem-20 87 91 ( ( PUNCT eurjchem-20 87 92 c‐2 c‐2 NOUN eurjchem-20 87 93 '' '' PUNCT eurjchem-20 87 94 , , PUNCT eurjchem-20 87 95     SPACE eurjchem-20 87 96 c‐6 c‐6 NOUN eurjchem-20 87 97 '' '' PUNCT eurjchem-20 87 98 ) ) PUNCT eurjchem-20 87 99 , , PUNCT eurjchem-20 87 100     SPACE eurjchem-20 87 101 111.1 111.1 NUM eurjchem-20 87 102     SPACE eurjchem-20 87 103 ( ( PUNCT eurjchem-20 87 104 c‐5 c‐5 NOUN eurjchem-20 87 105 ) ) PUNCT eurjchem-20 87 106 , , PUNCT eurjchem-20 87 107     SPACE eurjchem-20 87 108 89.8 89.8 NUM eurjchem-20 87 109     SPACE eurjchem-20 87 110 ( ( PUNCT eurjchem-20 87 111 c‐1 c‐1 NOUN eurjchem-20 87 112 ' ' PUNCT eurjchem-20 87 113 ) ) PUNCT eurjchem-20 87 114 , , PUNCT eurjchem-20 87 115     SPACE eurjchem-20 87 116 86.1 86.1 NUM eurjchem-20 87 117     SPACE eurjchem-20 87 118 ( ( PUNCT eurjchem-20 87 119 c‐ c‐ NOUN eurjchem-20 87 120 4 4 NUM eurjchem-20 87 121 ' ' NUM eurjchem-20 87 122 ) ) PUNCT eurjchem-20 87 123 , , PUNCT eurjchem-20 87 124     SPACE eurjchem-20 87 125 67.4 67.4 NUM eurjchem-20 87 126     SPACE eurjchem-20 87 127 ( ( PUNCT eurjchem-20 87 128 c‐5 c‐5 NOUN eurjchem-20 87 129 ' ' PUNCT eurjchem-20 87 130 ) ) PUNCT eurjchem-20 87 131 , , PUNCT eurjchem-20 87 132     SPACE eurjchem-20 87 133 61.1 61.1 NUM eurjchem-20 87 134     SPACE eurjchem-20 87 135 ( ( PUNCT eurjchem-20 87 136 o‐ch2 o‐ch2 PROPN eurjchem-20 87 137 ) ) PUNCT eurjchem-20 87 138 , , PUNCT eurjchem-20 87 139     SPACE eurjchem-20 87 140 53.7 53.7 NUM eurjchem-20 87 141     SPACE eurjchem-20 87 142 ( ( PUNCT eurjchem-20 87 143 cys‐ch cys‐ch PROPN eurjchem-20 87 144 ) ) PUNCT eurjchem-20 87 145 , , PUNCT eurjchem-20 87 146     SPACE eurjchem-20 87 147 22.1 22.1 NUM eurjchem-20 87 148     SPACE eurjchem-20 87 149 ( ( PUNCT eurjchem-20 87 150 cys‐ch2 cys‐ch2 PROPN eurjchem-20 87 151 ) ) PUNCT eurjchem-20 87 152 , , PUNCT eurjchem-20 87 153     SPACE eurjchem-20 87 154 13.8 13.8 NUM eurjchem-20 87 155     SPACE eurjchem-20 87 156 ( ( PUNCT eurjchem-20 87 157 ‐o‐ch2‐ch3 ‐o‐ch2‐ch3 ADJ eurjchem-20 87 158 ) ) PUNCT eurjchem-20 87 159 , , PUNCT eurjchem-20 87 160     SPACE eurjchem-20 87 161 12.1 12.1 NUM eurjchem-20 87 162     SPACE eurjchem-20 87 163 ( ( PUNCT eurjchem-20 87 164 ‐ch3 ‐ch3 ADJ eurjchem-20 87 165 ) ) PUNCT eurjchem-20 87 166 . . PUNCT eurjchem-20 87 167     SPACE eurjchem-20 88 1 31p‐nmr 31p‐nmr NOUN eurjchem-20 88 2     SPACE eurjchem-20 88 3 ( ( PUNCT eurjchem-20 88 4 202 202 NUM eurjchem-20 88 5     SPACE eurjchem-20 88 6 mhz mhz NOUN eurjchem-20 88 7 , , PUNCT eurjchem-20 88 8     SPACE eurjchem-20 88 9 dmso‐d6 dmso‐d6 NOUN eurjchem-20 88 10 , , PUNCT eurjchem-20 88 11     SPACE eurjchem-20 88 12   NUM eurjchem-20 88 13 ): ): PUNCT eurjchem-20 88 14     SPACE eurjchem-20 88 15 7.85 7.85 NUM eurjchem-20 88 16 . . PUNCT eurjchem-20 88 17             SPACE eurjchem-20 88 18 300 300 NUM eurjchem-20 88 19     SPACE eurjchem-20 88 20 rao rao PROPN eurjchem-20 88 21     SPACE eurjchem-20 88 22 et et PROPN eurjchem-20 88 23     SPACE eurjchem-20 88 24 al al PROPN eurjchem-20 88 25 . . PROPN eurjchem-20 88 26     SPACE eurjchem-20 88 27 / / SYM eurjchem-20 88 28     SPACE eurjchem-20 88 29 european european ADJ eurjchem-20 88 30     SPACE eurjchem-20 88 31 journal journal NOUN eurjchem-20 88 32     SPACE eurjchem-20 88 33 of of ADP eurjchem-20 88 34     SPACE eurjchem-20 88 35 chemistry chemistry NOUN eurjchem-20 88 36     SPACE eurjchem-20 88 37 1 1 NUM eurjchem-20 88 38     SPACE eurjchem-20 88 39 ( ( PUNCT eurjchem-20 88 40 4 4 NUM eurjchem-20 88 41 ) ) PUNCT eurjchem-20 88 42     SPACE eurjchem-20 88 43 ( ( PUNCT eurjchem-20 88 44 2010 2010 NUM eurjchem-20 88 45 ) ) PUNCT eurjchem-20 88 46     SPACE eurjchem-20 88 47 297­301 297­301 NUM eurjchem-20 88 48         SPACE eurjchem-20 88 49 table table NOUN eurjchem-20 88 50     SPACE eurjchem-20 88 51 1 1 NUM eurjchem-20 88 52 . . PUNCT eurjchem-20 88 53     SPACE eurjchem-20 88 54 antibacterial antibacterial ADJ eurjchem-20 88 55       SPACE eurjchem-20 88 56 activity activity NOUN eurjchem-20 88 57     SPACE eurjchem-20 88 58 of of ADP eurjchem-20 88 59     SPACE eurjchem-20 88 60 4a­l 4a­l PROPN eurjchem-20 88 61 . . PUNCT eurjchem-20 88 62     SPACE eurjchem-20 88 63 compounds compound VERB eurjchem-20 88 64     SPACE eurjchem-20 88 65 zone zone NOUN eurjchem-20 88 66     SPACE eurjchem-20 88 67 of of ADP eurjchem-20 88 68     SPACE eurjchem-20 88 69 inhibition inhibition NOUN eurjchem-20 88 70     SPACE eurjchem-20 88 71 in in ADP eurjchem-20 88 72     SPACE eurjchem-20 88 73 mm mm NOUN eurjchem-20 88 74     SPACE eurjchem-20 88 75 ( ( PUNCT eurjchem-20 88 76 100 100 NUM eurjchem-20 88 77     SPACE eurjchem-20 88 78 µg µg NOUN eurjchem-20 88 79 / / SYM eurjchem-20 88 80 ml ml NOUN eurjchem-20 88 81 ) ) PUNCT eurjchem-20 88 82     SPACE eurjchem-20 88 83 b. b. PROPN eurjchem-20 88 84     SPACE eurjchem-20 88 85 subtilis subtilis PROPN eurjchem-20 88 86     SPACE eurjchem-20 88 87 s. s. PROPN eurjchem-20 88 88     SPACE eurjchem-20 88 89 aureus aureus PROPN eurjchem-20 88 90 e. e. PROPN eurjchem-20 88 91     SPACE eurjchem-20 88 92 coli coli PROPN eurjchem-20 88 93 k. k. NOUN eurjchem-20 88 94     SPACE eurjchem-20 88 95 pneumoniae pneumoniae ADJ eurjchem-20 88 96 4a 4a NOUN eurjchem-20 88 97     SPACE eurjchem-20 88 98 12 12 NUM eurjchem-20 88 99     SPACE eurjchem-20 88 100 1 1 NUM eurjchem-20 88 101     SPACE eurjchem-20 88 102 0 0 NUM eurjchem-20 88 103 11 11 NUM eurjchem-20 88 104 10 10 NUM eurjchem-20 88 105 4b 4b NOUN eurjchem-20 88 106     SPACE eurjchem-20 88 107 12 12 NUM eurjchem-20 88 108     SPACE eurjchem-20 88 109 12 12 NUM eurjchem-20 88 110 10 10 NUM eurjchem-20 88 111 11 11 NUM eurjchem-20 88 112 4c 4c NOUN eurjchem-20 88 113     SPACE eurjchem-20 88 114 10 10 NUM eurjchem-20 88 115     SPACE eurjchem-20 88 116 10 10 NUM eurjchem-20 88 117 11 11 NUM eurjchem-20 88 118 13 13 NUM eurjchem-20 88 119 4d 4d NUM eurjchem-20 88 120     SPACE eurjchem-20 88 121 11 11 NUM eurjchem-20 88 122     SPACE eurjchem-20 88 123 13 13 NUM eurjchem-20 88 124 14 14 NUM eurjchem-20 88 125 12 12 NUM eurjchem-20 88 126 4e 4e NOUN eurjchem-20 88 127     SPACE eurjchem-20 88 128 ‐ ‐ NOUN eurjchem-20 88 129     SPACE eurjchem-20 88 130 ‐ ‐ NOUN eurjchem-20 88 131 9 9 NUM eurjchem-20 88 132 8 8 NUM eurjchem-20 88 133     SPACE eurjchem-20 88 134 4f 4f NUM eurjchem-20 88 135     SPACE eurjchem-20 88 136 12 12 NUM eurjchem-20 88 137     SPACE eurjchem-20 88 138 11 11 NUM eurjchem-20 88 139 16 16 NUM eurjchem-20 88 140 9 9 NUM eurjchem-20 88 141     SPACE eurjchem-20 88 142 4 4 NUM eurjchem-20 88 143 g g NOUN eurjchem-20 88 144     SPACE eurjchem-20 88 145 10 10 NUM eurjchem-20 88 146     SPACE eurjchem-20 88 147 8 8 NUM eurjchem-20 88 148 12 12 NUM eurjchem-20 88 149 10 10 NUM eurjchem-20 88 150 4h 4h NUM eurjchem-20 88 151     SPACE eurjchem-20 88 152 11 11 NUM eurjchem-20 88 153     SPACE eurjchem-20 88 154 9 9 NUM eurjchem-20 88 155 12 12 NUM eurjchem-20 88 156 11 11 NUM eurjchem-20 88 157 4i 4i NOUN eurjchem-20 88 158     SPACE eurjchem-20 88 159 13 13 NUM eurjchem-20 88 160     SPACE eurjchem-20 88 161 12 12 NUM eurjchem-20 88 162 13 13 NUM eurjchem-20 88 163 13 13 NUM eurjchem-20 88 164 4j 4j NOUN eurjchem-20 88 165     SPACE eurjchem-20 88 166 13 13 NUM eurjchem-20 88 167     SPACE eurjchem-20 88 168 11 11 NUM eurjchem-20 88 169 13 13 NUM eurjchem-20 88 170 14 14 NUM eurjchem-20 88 171 4k 4k NUM eurjchem-20 88 172     SPACE eurjchem-20 88 173 10 10 NUM eurjchem-20 88 174     SPACE eurjchem-20 88 175 15 15 NUM eurjchem-20 88 176 12 12 NUM eurjchem-20 88 177 11 11 NUM eurjchem-20 88 178 4l 4l NOUN eurjchem-20 88 179     SPACE eurjchem-20 88 180 11 11 NUM eurjchem-20 88 181     SPACE eurjchem-20 88 182 12 12 NUM eurjchem-20 88 183 17 17 NUM eurjchem-20 88 184 9 9 NUM eurjchem-20 88 185     SPACE eurjchem-20 88 186 ampicillin ampicillin NOUN eurjchem-20 88 187     SPACE eurjchem-20 88 188 11 11 NUM eurjchem-20 88 189     SPACE eurjchem-20 88 190 9 9 NUM eurjchem-20 88 191 13 13 NUM eurjchem-20 88 192 10 10 NUM eurjchem-20 88 193         SPACE eurjchem-20 88 194 2.2.11 2.2.11 NUM eurjchem-20 88 195 . . PUNCT eurjchem-20 88 196     SPACE eurjchem-20 88 197 benzyl1­((s)­((5­(5­methyl­2,4­dioxo­3,4­dihydro benzyl1­((s)­((5­(5­methyl­2,4­dioxo­3,4­dihydro NOUN eurjchem-20 88 198     SPACE eurjchem-20 88 199 pyrimidin­1(2h)­yl)­2,5­dihydrofuran­2­yl)methoxy pyrimidin­1(2h)­yl)­2,5­dihydrofuran­2­yl)methoxy PROPN eurjchem-20 88 200 ) ) PUNCT eurjchem-20 88 201     SPACE eurjchem-20 88 202 ( ( PUNCT eurjchem-20 88 203 4­ 4­ PROPN eurjchem-20 88 204 nitro­phenoxy nitro­phenoxy NOUN eurjchem-20 88 205 ) ) PUNCT eurjchem-20 88 206     SPACE eurjchem-20 88 207 phosphoryl)pyrrolidine­2­carboxylate phosphoryl)pyrrolidine­2­carboxylate NOUN eurjchem-20 88 208     SPACE eurjchem-20 88 209 ( ( PUNCT eurjchem-20 88 210 4k 4k NOUN eurjchem-20 88 211 ) ) PUNCT eurjchem-20 88 212         SPACE eurjchem-20 88 213 yield yield NOUN eurjchem-20 88 214 : : PUNCT eurjchem-20 88 215     SPACE eurjchem-20 88 216 62 62 NUM eurjchem-20 88 217     SPACE eurjchem-20 88 218 % % NOUN eurjchem-20 88 219 . . PUNCT eurjchem-20 88 220     SPACE eurjchem-20 89 1 m.p m.p PROPN eurjchem-20 89 2 . . PROPN eurjchem-20 89 3 : : PUNCT eurjchem-20 89 4     SPACE eurjchem-20 89 5 171‐173 171‐173 NUM eurjchem-20 89 6     SPACE eurjchem-20 89 7 oc oc PROPN eurjchem-20 89 8 . . PUNCT eurjchem-20 89 9     SPACE eurjchem-20 90 1 anal anal ADJ eurjchem-20 90 2 . . PUNCT eurjchem-20 90 3     SPACE eurjchem-20 90 4 calcd calcd NOUN eurjchem-20 90 5 . . PUNCT eurjchem-20 90 6     SPACE eurjchem-20 90 7 for for ADP eurjchem-20 90 8     SPACE eurjchem-20 90 9 c28h29n4o10p c28h29n4o10p NUM eurjchem-20 90 10 : : PUNCT eurjchem-20 90 11     SPACE eurjchem-20 90 12 c c X eurjchem-20 90 13 , , PUNCT eurjchem-20 90 14     SPACE eurjchem-20 90 15 54.90 54.90 NUM eurjchem-20 90 16 ; ; PUNCT eurjchem-20 90 17     SPACE eurjchem-20 90 18 h h NOUN eurjchem-20 90 19 , , PUNCT eurjchem-20 90 20     SPACE eurjchem-20 90 21 4.77 4.77 NUM eurjchem-20 90 22 ; ; PUNCT eurjchem-20 90 23     SPACE eurjchem-20 90 24 n n CCONJ eurjchem-20 90 25 , , PUNCT eurjchem-20 90 26     SPACE eurjchem-20 90 27 9.15 9.15 NUM eurjchem-20 90 28 ; ; PUNCT eurjchem-20 90 29     SPACE eurjchem-20 90 30 found find VERB eurjchem-20 90 31     SPACE eurjchem-20 90 32 c c NOUN eurjchem-20 90 33 , , PUNCT eurjchem-20 90 34     SPACE eurjchem-20 90 35 54.95 54.95 NUM eurjchem-20 90 36 ; ; PUNCT eurjchem-20 90 37     SPACE eurjchem-20 90 38 h h NOUN eurjchem-20 90 39 , , PUNCT eurjchem-20 90 40     SPACE eurjchem-20 90 41 4.79 4.79 NUM eurjchem-20 90 42 ; ; PUNCT eurjchem-20 90 43     SPACE eurjchem-20 90 44 n n CCONJ eurjchem-20 90 45 , , PUNCT eurjchem-20 90 46     SPACE eurjchem-20 90 47 9.11 9.11 NUM eurjchem-20 90 48 . . PUNCT eurjchem-20 90 49     SPACE eurjchem-20 91 1 ir ir PROPN eurjchem-20 91 2     SPACE eurjchem-20 91 3 ( ( PUNCT eurjchem-20 91 4 kbr kbr PROPN eurjchem-20 91 5 , , PUNCT eurjchem-20 91 6     SPACE eurjchem-20 91 7 cm‐1 cm‐1 PROPN eurjchem-20 91 8 ): ): PUNCT eurjchem-20 91 9     SPACE eurjchem-20 91 10 3379 3379 NUM eurjchem-20 91 11     SPACE eurjchem-20 91 12 ν(‐nh ν(‐nh PROPN eurjchem-20 91 13 ) ) PUNCT eurjchem-20 91 14 , , PUNCT eurjchem-20 91 15     SPACE eurjchem-20 91 16 1680 1680 NUM eurjchem-20 91 17 , , PUNCT eurjchem-20 91 18     SPACE eurjchem-20 91 19 1728 1728 NUM eurjchem-20 91 20     SPACE eurjchem-20 91 21 ν(c ν(c PROPN eurjchem-20 91 22 = = NOUN eurjchem-20 91 23 o o NOUN eurjchem-20 91 24 ) ) PUNCT eurjchem-20 91 25 , , PUNCT eurjchem-20 91 26     SPACE eurjchem-20 91 27 1234 1234 NUM eurjchem-20 91 28     SPACE eurjchem-20 91 29 ν(p ν(p PROPN eurjchem-20 91 30 = = SYM eurjchem-20 91 31 o o NOUN eurjchem-20 91 32 ) ) PUNCT eurjchem-20 91 33 . . PUNCT eurjchem-20 91 34     SPACE eurjchem-20 92 1 1h‐ 1h‐ NUM eurjchem-20 92 2 nmr nmr PROPN eurjchem-20 92 3     SPACE eurjchem-20 92 4 ( ( PUNCT eurjchem-20 92 5 500 500 NUM eurjchem-20 92 6     SPACE eurjchem-20 92 7 mhz mhz NOUN eurjchem-20 92 8 , , PUNCT eurjchem-20 92 9     SPACE eurjchem-20 92 10 dmso‐d6 dmso‐d6 NOUN eurjchem-20 92 11 , , PUNCT eurjchem-20 92 12     SPACE eurjchem-20 92 13   NUM eurjchem-20 92 14 ): ): PUNCT eurjchem-20 92 15     SPACE eurjchem-20 92 16 9.1 9.1 NUM eurjchem-20 92 17     SPACE eurjchem-20 92 18 ( ( PUNCT eurjchem-20 92 19 s s PROPN eurjchem-20 92 20 , , PUNCT eurjchem-20 92 21     SPACE eurjchem-20 92 22 1h 1h NUM eurjchem-20 92 23 , , PUNCT eurjchem-20 92 24     SPACE eurjchem-20 92 25 nh nh PROPN eurjchem-20 92 26 ) ) PUNCT eurjchem-20 92 27 , , PUNCT eurjchem-20 92 28       SPACE eurjchem-20 92 29 8.14 8.14 NUM eurjchem-20 92 30     SPACE eurjchem-20 92 31 ( ( PUNCT eurjchem-20 92 32 d d PROPN eurjchem-20 92 33 , , PUNCT eurjchem-20 92 34     SPACE eurjchem-20 92 35 2h 2h NUM eurjchem-20 92 36 , , PUNCT eurjchem-20 92 37     SPACE eurjchem-20 92 38 j=9.5 j=9.5 NOUN eurjchem-20 92 39     SPACE eurjchem-20 92 40 hz hz VERB eurjchem-20 92 41 , , PUNCT eurjchem-20 92 42     SPACE eurjchem-20 92 43 ar‐h ar‐h NOUN eurjchem-20 92 44 ) ) PUNCT eurjchem-20 92 45 , , PUNCT eurjchem-20 92 46     SPACE eurjchem-20 92 47 7.49 7.49 NUM eurjchem-20 92 48     SPACE eurjchem-20 92 49 ( ( PUNCT eurjchem-20 92 50 d d PROPN eurjchem-20 92 51 , , PUNCT eurjchem-20 92 52     SPACE eurjchem-20 92 53 1h 1h NUM eurjchem-20 92 54 , , PUNCT eurjchem-20 92 55     SPACE eurjchem-20 92 56 j=1.5 j=1.5 NOUN eurjchem-20 92 57     SPACE eurjchem-20 92 58 hz hz VERB eurjchem-20 92 59 , , PUNCT eurjchem-20 92 60     SPACE eurjchem-20 92 61 h‐6 h‐6 NOUN eurjchem-20 92 62 ) ) PUNCT eurjchem-20 92 63 , , PUNCT eurjchem-20 92 64     SPACE eurjchem-20 92 65 7.39 7.39 NUM eurjchem-20 92 66     SPACE eurjchem-20 92 67 ( ( PUNCT eurjchem-20 92 68 d d NOUN eurjchem-20 92 69 , , PUNCT eurjchem-20 92 70     SPACE eurjchem-20 92 71 2h 2h NUM eurjchem-20 92 72 , , PUNCT eurjchem-20 92 73     SPACE eurjchem-20 92 74 j=9 j=9 NOUN eurjchem-20 92 75     SPACE eurjchem-20 92 76 hz hz VERB eurjchem-20 92 77 , , PUNCT eurjchem-20 92 78     SPACE eurjchem-20 92 79 ar‐h ar‐h NOUN eurjchem-20 92 80 ) ) PUNCT eurjchem-20 92 81 , , PUNCT eurjchem-20 92 82     SPACE eurjchem-20 93 1 7.20‐7.32 7.20‐7.32 NUM eurjchem-20 93 2     SPACE eurjchem-20 93 3 ( ( PUNCT eurjchem-20 93 4 m m PROPN eurjchem-20 93 5 , , PUNCT eurjchem-20 93 6     SPACE eurjchem-20 93 7 5h 5h NUM eurjchem-20 93 8 , , PUNCT eurjchem-20 93 9     SPACE eurjchem-20 93 10 ar‐h ar‐h NOUN eurjchem-20 93 11 ) ) PUNCT eurjchem-20 93 12 , , PUNCT eurjchem-20 93 13     SPACE eurjchem-20 93 14 6.79‐6.80 6.79‐6.80 VERB eurjchem-20 93 15     SPACE eurjchem-20 93 16 ( ( PUNCT eurjchem-20 93 17 m m PROPN eurjchem-20 93 18 , , PUNCT eurjchem-20 93 19     SPACE eurjchem-20 93 20 1h 1h NUM eurjchem-20 93 21 , , PUNCT eurjchem-20 93 22     SPACE eurjchem-20 93 23 h‐1 h‐1 PROPN eurjchem-20 93 24 ' ' PUNCT eurjchem-20 93 25 ) ) PUNCT eurjchem-20 93 26 , , PUNCT eurjchem-20 93 27     SPACE eurjchem-20 93 28 6.33‐6.35 6.33‐6.35 NOUN eurjchem-20 93 29     SPACE eurjchem-20 93 30 ( ( PUNCT eurjchem-20 93 31 m m PROPN eurjchem-20 93 32 , , PUNCT eurjchem-20 93 33     SPACE eurjchem-20 93 34 1h 1h NUM eurjchem-20 93 35 , , PUNCT eurjchem-20 93 36     SPACE eurjchem-20 93 37 h‐2 h‐2 NOUN eurjchem-20 93 38 ' ' PUNCT eurjchem-20 93 39 ) ) PUNCT eurjchem-20 93 40 , , PUNCT eurjchem-20 93 41     SPACE eurjchem-20 93 42 5.90‐5.91 5.90‐5.91 NUM eurjchem-20 93 43     SPACE eurjchem-20 93 44 ( ( PUNCT eurjchem-20 93 45 m m PROPN eurjchem-20 93 46 , , PUNCT eurjchem-20 93 47     SPACE eurjchem-20 93 48 1h 1h NUM eurjchem-20 93 49 , , PUNCT eurjchem-20 93 50     SPACE eurjchem-20 93 51 h‐3 h‐3 NOUN eurjchem-20 93 52 ' ' PUNCT eurjchem-20 93 53 ) ) PUNCT eurjchem-20 93 54 , , PUNCT eurjchem-20 93 55     SPACE eurjchem-20 93 56 5.38 5.38 NUM eurjchem-20 93 57     SPACE eurjchem-20 93 58 ( ( PUNCT eurjchem-20 93 59 s s PROPN eurjchem-20 93 60 , , PUNCT eurjchem-20 93 61     SPACE eurjchem-20 93 62 2h 2h NUM eurjchem-20 93 63 , , PUNCT eurjchem-20 93 64     SPACE eurjchem-20 93 65 ph‐ch2 ph‐ch2 ADJ eurjchem-20 93 66 ) ) PUNCT eurjchem-20 93 67 , , PUNCT eurjchem-20 93 68     SPACE eurjchem-20 93 69 3.91‐ 3.91‐ NUM eurjchem-20 93 70 3.98 3.98 NUM eurjchem-20 93 71     SPACE eurjchem-20 93 72 ( ( PUNCT eurjchem-20 93 73 m m PROPN eurjchem-20 93 74 , , PUNCT eurjchem-20 93 75     SPACE eurjchem-20 93 76 4h 4h NOUN eurjchem-20 93 77 , , PUNCT eurjchem-20 93 78     SPACE eurjchem-20 93 79 2h‐5 2h‐5 NOUN eurjchem-20 93 80 ' ' PUNCT eurjchem-20 93 81 , , PUNCT eurjchem-20 93 82     SPACE eurjchem-20 93 83 h‐4 h‐4 NOUN eurjchem-20 93 84 ' ' PUNCT eurjchem-20 93 85 , , PUNCT eurjchem-20 93 86     SPACE eurjchem-20 93 87 prol‐ch prol‐ch NOUN eurjchem-20 93 88 ) ) PUNCT eurjchem-20 93 89 , , PUNCT eurjchem-20 93 90     SPACE eurjchem-20 93 91 2.83‐2.87 2.83‐2.87 NUM eurjchem-20 93 92     SPACE eurjchem-20 93 93 ( ( PUNCT eurjchem-20 93 94 m m PROPN eurjchem-20 93 95 , , PUNCT eurjchem-20 93 96     SPACE eurjchem-20 93 97 2h 2h NUM eurjchem-20 93 98 , , PUNCT eurjchem-20 93 99     SPACE eurjchem-20 93 100 n‐ch2 n‐ch2 NOUN eurjchem-20 93 101 ) ) PUNCT eurjchem-20 93 102 , , PUNCT eurjchem-20 93 103     SPACE eurjchem-20 93 104 1.92‐1.97 1.92‐1.97 NOUN eurjchem-20 93 105     SPACE eurjchem-20 93 106 ( ( PUNCT eurjchem-20 93 107 m m PROPN eurjchem-20 93 108 , , PUNCT eurjchem-20 93 109     SPACE eurjchem-20 93 110 4h 4h NOUN eurjchem-20 93 111 , , PUNCT eurjchem-20 93 112     SPACE eurjchem-20 93 113 ( ( PUNCT eurjchem-20 93 114 ch2)2 ch2)2 NOUN eurjchem-20 93 115 ) ) PUNCT eurjchem-20 93 116 , , PUNCT eurjchem-20 93 117     SPACE eurjchem-20 93 118 1.71 1.71 NUM eurjchem-20 93 119     SPACE eurjchem-20 93 120 ( ( PUNCT eurjchem-20 93 121 s s PROPN eurjchem-20 93 122 , , PUNCT eurjchem-20 93 123     SPACE eurjchem-20 93 124 3h 3h NUM eurjchem-20 93 125 , , PUNCT eurjchem-20 93 126     SPACE eurjchem-20 93 127 ch3 ch3 PROPN eurjchem-20 93 128 ) ) PUNCT eurjchem-20 93 129 , , PUNCT eurjchem-20 93 130     SPACE eurjchem-20 93 131 31p‐nmr 31p‐nmr NOUN eurjchem-20 93 132     SPACE eurjchem-20 93 133 ( ( PUNCT eurjchem-20 93 134 202 202 NUM eurjchem-20 93 135     SPACE eurjchem-20 93 136 mhz mhz NOUN eurjchem-20 93 137 , , PUNCT eurjchem-20 93 138     SPACE eurjchem-20 93 139 dmso‐d6 dmso‐d6 NOUN eurjchem-20 93 140 , , PUNCT eurjchem-20 93 141     SPACE eurjchem-20 93 142   NUM eurjchem-20 93 143 ): ): PUNCT eurjchem-20 93 144     SPACE eurjchem-20 93 145 2.12 2.12 NUM eurjchem-20 93 146 . . PUNCT eurjchem-20 93 147         SPACE eurjchem-20 93 148 2.2.12 2.2.12 NUM eurjchem-20 93 149 . . PUNCT eurjchem-20 93 150     SPACE eurjchem-20 94 1 methyl3­(1h­imidazol­4­yl)­2­((((2s,5r)­5­(5­methyl­ methyl3­(1h­imidazol­4­yl)­2­((((2s,5r)­5­(5­methyl­ PROPN eurjchem-20 94 2 2,4­dioxo­3,4dihydropyrimidin­1(2h)­yl)­2,5­dihydrofuran­ 2,4­dioxo­3,4dihydropyrimidin­1(2h)­yl)­2,5­dihydrofuran­ PROPN eurjchem-20 94 3 2­yl 2­yl NUM eurjchem-20 94 4 ) ) PUNCT eurjchem-20 94 5     SPACE eurjchem-20 94 6 methoxy methoxy NOUN eurjchem-20 94 7 ) ) PUNCT eurjchem-20 94 8     SPACE eurjchem-20 94 9 ( ( PUNCT eurjchem-20 94 10 4­nitrophenoxy)phosphorylamino 4­nitrophenoxy)phosphorylamino NUM eurjchem-20 94 11 ) ) PUNCT eurjchem-20 94 12     SPACE eurjchem-20 94 13 propanoate propanoate NOUN eurjchem-20 94 14     SPACE eurjchem-20 94 15 ( ( PUNCT eurjchem-20 94 16 4l 4l NOUN eurjchem-20 94 17 ) ) PUNCT eurjchem-20 94 18         SPACE eurjchem-20 94 19 yield yield NOUN eurjchem-20 94 20 : : PUNCT eurjchem-20 94 21     SPACE eurjchem-20 94 22 65 65 NUM eurjchem-20 94 23     SPACE eurjchem-20 94 24 % % NOUN eurjchem-20 94 25 . . PUNCT eurjchem-20 94 26     SPACE eurjchem-20 95 1 m.p m.p PROPN eurjchem-20 95 2 . . PROPN eurjchem-20 95 3 : : PUNCT eurjchem-20 95 4     SPACE eurjchem-20 95 5 164‐167 164‐167 NUM eurjchem-20 95 6     SPACE eurjchem-20 95 7 oc oc PROPN eurjchem-20 95 8 , , PUNCT eurjchem-20 95 9     SPACE eurjchem-20 95 10 anal anal ADJ eurjchem-20 95 11 . . PUNCT eurjchem-20 95 12     SPACE eurjchem-20 95 13 calcd calcd NOUN eurjchem-20 95 14 . . PUNCT eurjchem-20 95 15     SPACE eurjchem-20 95 16 for for ADP eurjchem-20 95 17     SPACE eurjchem-20 95 18 c23h25n6o10p c23h25n6o10p NOUN eurjchem-20 95 19 : : PUNCT eurjchem-20 95 20     SPACE eurjchem-20 95 21 c c NOUN eurjchem-20 95 22 , , PUNCT eurjchem-20 95 23     SPACE eurjchem-20 95 24 47.92 47.92 NUM eurjchem-20 95 25 ; ; PUNCT eurjchem-20 95 26     SPACE eurjchem-20 95 27 h h NOUN eurjchem-20 95 28 , , PUNCT eurjchem-20 95 29     SPACE eurjchem-20 95 30 4.37 4.37 NUM eurjchem-20 95 31 ; ; PUNCT eurjchem-20 95 32     SPACE eurjchem-20 95 33 n n CCONJ eurjchem-20 95 34 , , PUNCT eurjchem-20 95 35     SPACE eurjchem-20 95 36 14.58 14.58 NUM eurjchem-20 95 37 ; ; PUNCT eurjchem-20 95 38     SPACE eurjchem-20 95 39 found find VERB eurjchem-20 95 40     SPACE eurjchem-20 95 41 c c NOUN eurjchem-20 95 42 , , PUNCT eurjchem-20 95 43     SPACE eurjchem-20 95 44 47.87 47.87 NUM eurjchem-20 95 45 ; ; PUNCT eurjchem-20 95 46     SPACE eurjchem-20 95 47 h h NOUN eurjchem-20 95 48 , , PUNCT eurjchem-20 95 49     SPACE eurjchem-20 95 50 4.34 4.34 NUM eurjchem-20 95 51 ; ; PUNCT eurjchem-20 95 52     SPACE eurjchem-20 95 53 n n CCONJ eurjchem-20 95 54 , , PUNCT eurjchem-20 95 55     SPACE eurjchem-20 95 56 14.65 14.65 NUM eurjchem-20 95 57 . . PUNCT eurjchem-20 95 58     SPACE eurjchem-20 96 1 ir ir PROPN eurjchem-20 96 2     SPACE eurjchem-20 96 3 ( ( PUNCT eurjchem-20 96 4 kbr kbr PROPN eurjchem-20 96 5 , , PUNCT eurjchem-20 96 6     SPACE eurjchem-20 96 7 cm‐1 cm‐1 NOUN eurjchem-20 96 8 ): ): PUNCT eurjchem-20 96 9     SPACE eurjchem-20 96 10 3385 3385 NUM eurjchem-20 96 11     SPACE eurjchem-20 96 12 ν(‐nh ν(‐nh PROPN eurjchem-20 96 13 ) ) PUNCT eurjchem-20 96 14 , , PUNCT eurjchem-20 96 15     SPACE eurjchem-20 96 16 1680 1680 NUM eurjchem-20 96 17 , , PUNCT eurjchem-20 96 18     SPACE eurjchem-20 96 19 1731 1731 NUM eurjchem-20 96 20     SPACE eurjchem-20 96 21 ν(c ν(c PROPN eurjchem-20 96 22 = = SYM eurjchem-20 96 23 o o NOUN eurjchem-20 96 24 ) ) PUNCT eurjchem-20 96 25 , , PUNCT eurjchem-20 96 26     SPACE eurjchem-20 96 27 1226 1226 NUM eurjchem-20 96 28     SPACE eurjchem-20 96 29 ν(p ν(p NOUN eurjchem-20 96 30 = = SYM eurjchem-20 96 31 o o NOUN eurjchem-20 96 32 ) ) PUNCT eurjchem-20 96 33 . . PUNCT eurjchem-20 96 34     SPACE eurjchem-20 97 1 1h‐ 1h‐ NUM eurjchem-20 97 2 nmr nmr PROPN eurjchem-20 97 3     SPACE eurjchem-20 97 4 ( ( PUNCT eurjchem-20 97 5 500 500 NUM eurjchem-20 97 6     SPACE eurjchem-20 97 7 mhz mhz NOUN eurjchem-20 97 8 , , PUNCT eurjchem-20 97 9     SPACE eurjchem-20 97 10 dmso‐d6 dmso‐d6 NOUN eurjchem-20 97 11 , , PUNCT eurjchem-20 97 12     SPACE eurjchem-20 97 13   NUM eurjchem-20 97 14 ): ): PUNCT eurjchem-20 97 15     SPACE eurjchem-20 97 16 11.2 11.2 NUM eurjchem-20 97 17     SPACE eurjchem-20 97 18 ( ( PUNCT eurjchem-20 97 19 br br NOUN eurjchem-20 97 20     SPACE eurjchem-20 97 21 s s PROPN eurjchem-20 97 22 , , PUNCT eurjchem-20 97 23     SPACE eurjchem-20 97 24 1h 1h NUM eurjchem-20 97 25 , , PUNCT eurjchem-20 97 26     SPACE eurjchem-20 97 27 nh nh PROPN eurjchem-20 97 28 ) ) PUNCT eurjchem-20 97 29 , , PUNCT eurjchem-20 97 30     SPACE eurjchem-20 97 31 9.2 9.2 NUM eurjchem-20 97 32     SPACE eurjchem-20 97 33 ( ( PUNCT eurjchem-20 97 34 s s PROPN eurjchem-20 97 35 , , PUNCT eurjchem-20 97 36     SPACE eurjchem-20 97 37 1h 1h NUM eurjchem-20 97 38 , , PUNCT eurjchem-20 97 39     SPACE eurjchem-20 97 40 nh nh PROPN eurjchem-20 97 41 ) ) PUNCT eurjchem-20 97 42 , , PUNCT eurjchem-20 97 43     SPACE eurjchem-20 97 44 8.65‐8.67 8.65‐8.67 NUM eurjchem-20 97 45     SPACE eurjchem-20 97 46 ( ( PUNCT eurjchem-20 97 47 m m PROPN eurjchem-20 97 48 , , PUNCT eurjchem-20 97 49     SPACE eurjchem-20 97 50 1h 1h NUM eurjchem-20 97 51 , , PUNCT eurjchem-20 97 52     SPACE eurjchem-20 97 53 n n CCONJ eurjchem-20 97 54 = = NOUN eurjchem-20 97 55 ch ch NOUN eurjchem-20 97 56 ) ) PUNCT eurjchem-20 97 57 , , PUNCT eurjchem-20 97 58     SPACE eurjchem-20 97 59 8.21 8.21 NUM eurjchem-20 97 60     SPACE eurjchem-20 97 61 ( ( PUNCT eurjchem-20 97 62 d d PROPN eurjchem-20 97 63 , , PUNCT eurjchem-20 97 64     SPACE eurjchem-20 97 65 2h 2h NUM eurjchem-20 97 66 , , PUNCT eurjchem-20 97 67     SPACE eurjchem-20 97 68 j=9.5 j=9.5 NOUN eurjchem-20 97 69     SPACE eurjchem-20 97 70 hz hz VERB eurjchem-20 97 71 , , PUNCT eurjchem-20 97 72     SPACE eurjchem-20 97 73 ar‐h ar‐h NOUN eurjchem-20 97 74 ) ) PUNCT eurjchem-20 97 75 , , PUNCT eurjchem-20 97 76     SPACE eurjchem-20 97 77 7.51 7.51 NUM eurjchem-20 97 78     SPACE eurjchem-20 97 79 ( ( PUNCT eurjchem-20 97 80 d d PROPN eurjchem-20 97 81 , , PUNCT eurjchem-20 97 82     SPACE eurjchem-20 97 83 1h 1h NUM eurjchem-20 97 84 , , PUNCT eurjchem-20 97 85     SPACE eurjchem-20 97 86 j=1 j=1 NOUN eurjchem-20 97 87     SPACE eurjchem-20 97 88 hz hz VERB eurjchem-20 97 89 , , PUNCT eurjchem-20 97 90     SPACE eurjchem-20 97 91 h‐6 h‐6 NOUN eurjchem-20 97 92 ) ) PUNCT eurjchem-20 97 93 , , PUNCT eurjchem-20 97 94     SPACE eurjchem-20 98 1 7.38‐7.44 7.38‐7.44 NOUN eurjchem-20 98 2     SPACE eurjchem-20 98 3 ( ( PUNCT eurjchem-20 98 4 m m PROPN eurjchem-20 98 5 , , PUNCT eurjchem-20 98 6     SPACE eurjchem-20 98 7 3h 3h NUM eurjchem-20 98 8 , , PUNCT eurjchem-20 98 9     SPACE eurjchem-20 98 10 nh‐ch nh‐ch NUM eurjchem-20 98 11 , , PUNCT eurjchem-20 98 12     SPACE eurjchem-20 98 13 2ar‐h 2ar‐h NUM eurjchem-20 98 14 ) ) PUNCT eurjchem-20 98 15 , , PUNCT eurjchem-20 98 16     SPACE eurjchem-20 98 17 6.8‐6.81 6.8‐6.81 NUM eurjchem-20 98 18     SPACE eurjchem-20 98 19 ( ( PUNCT eurjchem-20 98 20 m m PROPN eurjchem-20 98 21 , , PUNCT eurjchem-20 98 22     SPACE eurjchem-20 98 23 1h 1h NUM eurjchem-20 98 24 , , PUNCT eurjchem-20 98 25     SPACE eurjchem-20 98 26 h‐1 h‐1 PROPN eurjchem-20 98 27 ' ' PUNCT eurjchem-20 98 28 ) ) PUNCT eurjchem-20 98 29 , , PUNCT eurjchem-20 98 30     SPACE eurjchem-20 98 31 6.32‐6.34 6.32‐6.34 PROPN eurjchem-20 98 32     SPACE eurjchem-20 98 33 ( ( PUNCT eurjchem-20 98 34 m m PROPN eurjchem-20 98 35 , , PUNCT eurjchem-20 98 36     SPACE eurjchem-20 98 37 1h 1h NUM eurjchem-20 98 38 , , PUNCT eurjchem-20 98 39     SPACE eurjchem-20 98 40 h‐2 h‐2 NOUN eurjchem-20 98 41 ' ' PUNCT eurjchem-20 98 42 ) ) PUNCT eurjchem-20 98 43 , , PUNCT eurjchem-20 98 44     SPACE eurjchem-20 98 45 5.89‐5.90 5.89‐5.90 NUM eurjchem-20 98 46     SPACE eurjchem-20 98 47 ( ( PUNCT eurjchem-20 98 48 m m PROPN eurjchem-20 98 49 , , PUNCT eurjchem-20 98 50     SPACE eurjchem-20 98 51 1h 1h NUM eurjchem-20 98 52 , , PUNCT eurjchem-20 98 53     SPACE eurjchem-20 98 54 h‐3 h‐3 NOUN eurjchem-20 98 55 ' ' PUNCT eurjchem-20 98 56 ) ) PUNCT eurjchem-20 98 57 , , PUNCT eurjchem-20 98 58     SPACE eurjchem-20 98 59 5.2 5.2 NUM eurjchem-20 98 60     SPACE eurjchem-20 98 61 ( ( PUNCT eurjchem-20 98 62 brs br VERB eurjchem-20 98 63 , , PUNCT eurjchem-20 98 64     SPACE eurjchem-20 98 65 1h 1h NUM eurjchem-20 98 66 , , PUNCT eurjchem-20 98 67     SPACE eurjchem-20 98 68 ‐nh ‐nh NOUN eurjchem-20 98 69 ) ) PUNCT eurjchem-20 98 70 , , PUNCT eurjchem-20 98 71     SPACE eurjchem-20 98 72 3.96‐4.04 3.96‐4.04 NOUN eurjchem-20 98 73     SPACE eurjchem-20 98 74 ( ( PUNCT eurjchem-20 98 75 m m PROPN eurjchem-20 98 76 , , PUNCT eurjchem-20 98 77     SPACE eurjchem-20 98 78 4h 4h NOUN eurjchem-20 98 79 , , PUNCT eurjchem-20 98 80     SPACE eurjchem-20 98 81 2h‐5 2h‐5 NOUN eurjchem-20 98 82 ' ' PUNCT eurjchem-20 98 83 , , PUNCT eurjchem-20 98 84     SPACE eurjchem-20 98 85 h‐4 h‐4 NOUN eurjchem-20 98 86 ' ' PART eurjchem-20 98 87 , , PUNCT eurjchem-20 98 88     SPACE eurjchem-20 98 89 his‐ch his‐ch PROPN eurjchem-20 98 90 ) ) PUNCT eurjchem-20 98 91 , , PUNCT eurjchem-20 98 92     SPACE eurjchem-20 98 93 3.34‐3.38 3.34‐3.38 NUM eurjchem-20 98 94     SPACE eurjchem-20 98 95 ( ( PUNCT eurjchem-20 98 96 m,2h m,2h PROPN eurjchem-20 98 97 , , PUNCT eurjchem-20 98 98     SPACE eurjchem-20 98 99 his‐ch2 his‐ch2 NOUN eurjchem-20 98 100 ) ) PUNCT eurjchem-20 98 101 , , PUNCT eurjchem-20 98 102     SPACE eurjchem-20 98 103 3.21 3.21 NUM eurjchem-20 98 104     SPACE eurjchem-20 98 105 ( ( PUNCT eurjchem-20 98 106 s s PROPN eurjchem-20 98 107 , , PUNCT eurjchem-20 98 108     SPACE eurjchem-20 98 109 3h 3h NUM eurjchem-20 98 110 , , PUNCT eurjchem-20 98 111     SPACE eurjchem-20 98 112 ‐och3 ‐och3 NOUN eurjchem-20 98 113 ) ) PUNCT eurjchem-20 98 114 . . PUNCT eurjchem-20 98 115     SPACE eurjchem-20 99 1 31p‐nmr 31p‐nmr NOUN eurjchem-20 99 2     SPACE eurjchem-20 99 3 ( ( PUNCT eurjchem-20 99 4 202 202 NUM eurjchem-20 99 5     SPACE eurjchem-20 99 6 mhz mhz NOUN eurjchem-20 99 7 , , PUNCT eurjchem-20 99 8     SPACE eurjchem-20 99 9 dmso‐ dmso‐ PROPN eurjchem-20 99 10 d6 d6 NOUN eurjchem-20 99 11 , , PUNCT eurjchem-20 99 12     SPACE eurjchem-20 99 13   NUM eurjchem-20 99 14 ): ): PUNCT eurjchem-20 99 15     SPACE eurjchem-20 99 16 3.31 3.31 NUM eurjchem-20 99 17 . . PUNCT eurjchem-20 99 18         SPACE eurjchem-20 99 19 2.3 2.3 NUM eurjchem-20 99 20 . . PUNCT eurjchem-20 99 21     SPACE eurjchem-20 99 22 biological biological ADJ eurjchem-20 99 23     SPACE eurjchem-20 99 24 activity activity NOUN eurjchem-20 99 25         SPACE eurjchem-20 99 26 2.3.1 2.3.1 NUM eurjchem-20 99 27 . . PUNCT eurjchem-20 99 28     SPACE eurjchem-20 99 29 antibacterial antibacterial ADJ eurjchem-20 99 30     SPACE eurjchem-20 99 31 activity activity NOUN eurjchem-20 99 32         SPACE eurjchem-20 99 33 compounds compound VERB eurjchem-20 99 34     SPACE eurjchem-20 99 35 4a­l 4a­l NOUN eurjchem-20 99 36     SPACE eurjchem-20 99 37 were be AUX eurjchem-20 99 38     SPACE eurjchem-20 99 39 screened screen VERB eurjchem-20 99 40     SPACE eurjchem-20 99 41 for for ADP eurjchem-20 99 42     SPACE eurjchem-20 99 43 their their PRON eurjchem-20 99 44     SPACE eurjchem-20 99 45 antibacterial antibacterial ADJ eurjchem-20 99 46     SPACE eurjchem-20 99 47 activity activity NOUN eurjchem-20 99 48     SPACE eurjchem-20 99 49 against against ADP eurjchem-20 99 50     SPACE eurjchem-20 99 51 gram gram NOUN eurjchem-20 99 52     SPACE eurjchem-20 99 53 positive positive ADJ eurjchem-20 99 54     SPACE eurjchem-20 99 55 bacteria bacteria NOUN eurjchem-20 99 56 , , PUNCT eurjchem-20 99 57     SPACE eurjchem-20 99 58 staphylococcus staphylococcus NOUN eurjchem-20 99 59     SPACE eurjchem-20 99 60 aureus aureus NOUN eurjchem-20 99 61 , , PUNCT eurjchem-20 99 62     SPACE eurjchem-20 99 63 bacillus bacillus NOUN eurjchem-20 99 64     SPACE eurjchem-20 99 65 subtilis subtili NOUN eurjchem-20 99 66     SPACE eurjchem-20 99 67 and and CCONJ eurjchem-20 99 68     SPACE eurjchem-20 99 69 gram gram NOUN eurjchem-20 99 70     SPACE eurjchem-20 99 71 negative negative ADJ eurjchem-20 99 72     SPACE eurjchem-20 99 73 bacteria bacteria NOUN eurjchem-20 99 74 , , PUNCT eurjchem-20 99 75     SPACE eurjchem-20 99 76 escherichia escherichia NOUN eurjchem-20 99 77     SPACE eurjchem-20 99 78 coli coli NOUN eurjchem-20 99 79 , , PUNCT eurjchem-20 99 80     SPACE eurjchem-20 99 81 klebsiella klebsiella NOUN eurjchem-20 99 82     SPACE eurjchem-20 99 83 pneumoniae pneumoniae NOUN eurjchem-20 99 84     SPACE eurjchem-20 99 85 by by ADP eurjchem-20 99 86     SPACE eurjchem-20 99 87 the the DET eurjchem-20 99 88     SPACE eurjchem-20 99 89 cup cup NOUN eurjchem-20 99 90     SPACE eurjchem-20 99 91 plate plate NOUN eurjchem-20 99 92     SPACE eurjchem-20 99 93 method method NOUN eurjchem-20 99 94     SPACE eurjchem-20 100 1 [ [ X eurjchem-20 100 2 12 12 NUM eurjchem-20 100 3 ] ] PUNCT eurjchem-20 100 4     SPACE eurjchem-20 100 5 in in ADP eurjchem-20 100 6     SPACE eurjchem-20 100 7 nutrient nutrient NOUN eurjchem-20 100 8     SPACE eurjchem-20 100 9 agar agar NOUN eurjchem-20 100 10     SPACE eurjchem-20 100 11 medium medium NOUN eurjchem-20 100 12     SPACE eurjchem-20 100 13 at at ADP eurjchem-20 100 14     SPACE eurjchem-20 100 15 the the DET eurjchem-20 100 16     SPACE eurjchem-20 100 17 concentration concentration NOUN eurjchem-20 100 18     SPACE eurjchem-20 100 19 of of ADP eurjchem-20 100 20     SPACE eurjchem-20 100 21 100 100 NUM eurjchem-20 100 22     SPACE eurjchem-20 100 23 µg µg VERB eurjchem-20 100 24 / / SYM eurjchem-20 100 25 ml ml VERB eurjchem-20 100 26     SPACE eurjchem-20 100 27 in in ADP eurjchem-20 100 28     SPACE eurjchem-20 100 29 dmso dmso NOUN eurjchem-20 100 30 . . PUNCT eurjchem-20 100 31     SPACE eurjchem-20 100 32 nutrient nutrient NOUN eurjchem-20 100 33     SPACE eurjchem-20 100 34 agar agar NOUN eurjchem-20 100 35     SPACE eurjchem-20 100 36 plates plate NOUN eurjchem-20 100 37     SPACE eurjchem-20 100 38 were be AUX eurjchem-20 100 39     SPACE eurjchem-20 100 40 prepared prepare VERB eurjchem-20 100 41     SPACE eurjchem-20 100 42 by by ADP eurjchem-20 100 43     SPACE eurjchem-20 100 44 pouring pour VERB eurjchem-20 100 45     SPACE eurjchem-20 100 46 20 20 NUM eurjchem-20 100 47     SPACE eurjchem-20 100 48 ml ml NOUN eurjchem-20 100 49     SPACE eurjchem-20 100 50 of of ADP eurjchem-20 100 51     SPACE eurjchem-20 100 52 nutrient nutrient NOUN eurjchem-20 100 53     SPACE eurjchem-20 100 54 agar agar NOUN eurjchem-20 100 55     SPACE eurjchem-20 100 56 in in ADP eurjchem-20 100 57     SPACE eurjchem-20 100 58 sterile sterile ADJ eurjchem-20 100 59     SPACE eurjchem-20 100 60 petri petri ADJ eurjchem-20 100 61     SPACE eurjchem-20 100 62 dishes dish NOUN eurjchem-20 100 63     SPACE eurjchem-20 100 64 for for ADP eurjchem-20 100 65     SPACE eurjchem-20 100 66 antibacterial antibacterial ADJ eurjchem-20 100 67     SPACE eurjchem-20 100 68 assay assay NOUN eurjchem-20 100 69 . . PUNCT eurjchem-20 100 70     SPACE eurjchem-20 101 1 concentration concentration NOUN eurjchem-20 101 2     SPACE eurjchem-20 101 3 of of ADP eurjchem-20 101 4     SPACE eurjchem-20 101 5 these these DET eurjchem-20 101 6     SPACE eurjchem-20 101 7 organisms organism NOUN eurjchem-20 101 8     SPACE eurjchem-20 101 9 was be AUX eurjchem-20 101 10     SPACE eurjchem-20 101 11 prepared prepare VERB eurjchem-20 101 12     SPACE eurjchem-20 101 13 to to PART eurjchem-20 101 14     SPACE eurjchem-20 101 15 contain contain VERB eurjchem-20 101 16     SPACE eurjchem-20 101 17 approximately approximately ADV eurjchem-20 101 18     SPACE eurjchem-20 101 19 1×106 1×106 NUM eurjchem-20 101 20     SPACE eurjchem-20 101 21 cfu cfu NOUN eurjchem-20 101 22 / / SYM eurjchem-20 101 23 ml ml NOUN eurjchem-20 101 24 . . PUNCT eurjchem-20 101 25     SPACE eurjchem-20 101 26 the the DET eurjchem-20 101 27     SPACE eurjchem-20 101 28 tubes tube NOUN eurjchem-20 101 29     SPACE eurjchem-20 101 30 were be AUX eurjchem-20 101 31     SPACE eurjchem-20 101 32 then then ADV eurjchem-20 101 33     SPACE eurjchem-20 101 34 inoculated inoculate VERB eurjchem-20 101 35     SPACE eurjchem-20 101 36 with with ADP eurjchem-20 101 37     SPACE eurjchem-20 101 38 0.1 0.1 NUM eurjchem-20 101 39     SPACE eurjchem-20 101 40 ml ml NOUN eurjchem-20 101 41     SPACE eurjchem-20 101 42 of of ADP eurjchem-20 101 43     SPACE eurjchem-20 101 44 the the DET eurjchem-20 101 45     SPACE eurjchem-20 101 46 appropriate appropriate ADJ eurjchem-20 101 47     SPACE eurjchem-20 101 48 culture culture NOUN eurjchem-20 101 49     SPACE eurjchem-20 101 50 suspension suspension NOUN eurjchem-20 101 51     SPACE eurjchem-20 101 52 of of ADP eurjchem-20 101 53     SPACE eurjchem-20 101 54 bacterium bacterium NOUN eurjchem-20 101 55     SPACE eurjchem-20 101 56 mixed mixed ADJ eurjchem-20 101 57     SPACE eurjchem-20 101 58 gently gently ADV eurjchem-20 101 59     SPACE eurjchem-20 101 60 and and CCONJ eurjchem-20 101 61     SPACE eurjchem-20 101 62 poured pour VERB eurjchem-20 101 63     SPACE eurjchem-20 101 64 onto onto AUX eurjchem-20 101 65     SPACE eurjchem-20 101 66 previously previously ADV eurjchem-20 101 67     SPACE eurjchem-20 101 68 solidified solidify VERB eurjchem-20 101 69     SPACE eurjchem-20 101 70 nutrient nutrient NOUN eurjchem-20 101 71     SPACE eurjchem-20 101 72 agar agar NOUN eurjchem-20 101 73 . . PUNCT eurjchem-20 101 74     SPACE eurjchem-20 101 75 after after ADP eurjchem-20 101 76     SPACE eurjchem-20 101 77 setting setting NOUN eurjchem-20 101 78 , , PUNCT eurjchem-20 101 79     SPACE eurjchem-20 101 80 a a DET eurjchem-20 101 81     SPACE eurjchem-20 101 82 cup cup NOUN eurjchem-20 101 83     SPACE eurjchem-20 101 84 borer borer NOUN eurjchem-20 101 85     SPACE eurjchem-20 101 86 ( ( PUNCT eurjchem-20 101 87 6 6 NUM eurjchem-20 101 88     SPACE eurjchem-20 101 89 mm mm NUM eurjchem-20 101 90     SPACE eurjchem-20 101 91 diameter diameter NOUN eurjchem-20 101 92 ) ) PUNCT eurjchem-20 101 93     SPACE eurjchem-20 101 94 was be AUX eurjchem-20 101 95     SPACE eurjchem-20 101 96 properly properly ADV eurjchem-20 101 97     SPACE eurjchem-20 101 98 sterilized sterilize VERB eurjchem-20 101 99     SPACE eurjchem-20 101 100 by by ADP eurjchem-20 101 101     SPACE eurjchem-20 101 102 flaming flame VERB eurjchem-20 101 103     SPACE eurjchem-20 101 104 and and CCONJ eurjchem-20 101 105     SPACE eurjchem-20 101 106 used use VERB eurjchem-20 101 107     SPACE eurjchem-20 101 108 to to PART eurjchem-20 101 109     SPACE eurjchem-20 101 110 make make VERB eurjchem-20 101 111     SPACE eurjchem-20 101 112 four four NUM eurjchem-20 101 113     SPACE eurjchem-20 101 114 uniform uniform NOUN eurjchem-20 101 115     SPACE eurjchem-20 101 116 cups cup NOUN eurjchem-20 101 117     SPACE eurjchem-20 101 118 in in ADP eurjchem-20 101 119     SPACE eurjchem-20 101 120 each each DET eurjchem-20 101 121     SPACE eurjchem-20 101 122 petri petri ADJ eurjchem-20 101 123     SPACE eurjchem-20 101 124 dish dish NOUN eurjchem-20 101 125 . . PUNCT eurjchem-20 101 126     SPACE eurjchem-20 102 1 the the DET eurjchem-20 102 2     SPACE eurjchem-20 102 3 cups cup NOUN eurjchem-20 102 4     SPACE eurjchem-20 102 5 were be AUX eurjchem-20 102 6     SPACE eurjchem-20 102 7 then then ADV eurjchem-20 102 8     SPACE eurjchem-20 102 9 filled fill VERB eurjchem-20 102 10     SPACE eurjchem-20 102 11 with with ADP eurjchem-20 102 12     SPACE eurjchem-20 102 13 the the DET eurjchem-20 102 14     SPACE eurjchem-20 102 15 test test NOUN eurjchem-20 102 16     SPACE eurjchem-20 102 17 compounds compound VERB eurjchem-20 102 18     SPACE eurjchem-20 102 19 and and CCONJ eurjchem-20 102 20     SPACE eurjchem-20 102 21 allowed allow VERB eurjchem-20 102 22     SPACE eurjchem-20 102 23 to to PART eurjchem-20 102 24     SPACE eurjchem-20 102 25 diffuse diffuse VERB eurjchem-20 102 26     SPACE eurjchem-20 102 27 for for ADP eurjchem-20 102 28     SPACE eurjchem-20 102 29 45 45 NUM eurjchem-20 102 30     SPACE eurjchem-20 102 31 minutes minute NOUN eurjchem-20 102 32 . . PUNCT eurjchem-20 102 33     SPACE eurjchem-20 103 1 ampicillin ampicillin PROPN eurjchem-20 103 2     SPACE eurjchem-20 103 3 ( ( PUNCT eurjchem-20 103 4 100 100 NUM eurjchem-20 103 5     SPACE eurjchem-20 103 6 μg μg NOUN eurjchem-20 103 7 / / SYM eurjchem-20 103 8 disc disc PROPN eurjchem-20 103 9 ) ) PUNCT eurjchem-20 103 10     SPACE eurjchem-20 103 11 was be AUX eurjchem-20 103 12     SPACE eurjchem-20 103 13 used use VERB eurjchem-20 103 14     SPACE eurjchem-20 103 15 as as ADP eurjchem-20 103 16     SPACE eurjchem-20 103 17 standard standard NOUN eurjchem-20 103 18     SPACE eurjchem-20 103 19 for for ADP eurjchem-20 103 20     SPACE eurjchem-20 103 21 bacteria bacteria NOUN eurjchem-20 103 22 . . PUNCT eurjchem-20 103 23     SPACE eurjchem-20 104 1 the the DET eurjchem-20 104 2     SPACE eurjchem-20 104 3 plates plate NOUN eurjchem-20 104 4     SPACE eurjchem-20 104 5 were be AUX eurjchem-20 104 6     SPACE eurjchem-20 104 7 incubated incubate VERB eurjchem-20 104 8     SPACE eurjchem-20 104 9 at at ADP eurjchem-20 104 10     SPACE eurjchem-20 104 11 37 37 NUM eurjchem-20 104 12     SPACE eurjchem-20 104 13 oc oc NOUN eurjchem-20 104 14     SPACE eurjchem-20 104 15 for for ADP eurjchem-20 104 16     SPACE eurjchem-20 104 17 24 24 NUM eurjchem-20 104 18     SPACE eurjchem-20 104 19 hours hour NOUN eurjchem-20 104 20 . . PUNCT eurjchem-20 104 21     SPACE eurjchem-20 104 22 at at ADP eurjchem-20 104 23     SPACE eurjchem-20 104 24 the the DET eurjchem-20 104 25     SPACE eurjchem-20 104 26 end end NOUN eurjchem-20 104 27     SPACE eurjchem-20 104 28 of of ADP eurjchem-20 104 29     SPACE eurjchem-20 104 30 the the DET eurjchem-20 104 31     SPACE eurjchem-20 104 32 period period NOUN eurjchem-20 104 33 , , PUNCT eurjchem-20 104 34     SPACE eurjchem-20 104 35 inhibition inhibition NOUN eurjchem-20 104 36     SPACE eurjchem-20 104 37 zones zone NOUN eurjchem-20 104 38     SPACE eurjchem-20 104 39 formed form VERB eurjchem-20 104 40     SPACE eurjchem-20 104 41 on on ADP eurjchem-20 104 42     SPACE eurjchem-20 104 43 the the DET eurjchem-20 104 44     SPACE eurjchem-20 104 45 medium medium NOUN eurjchem-20 104 46     SPACE eurjchem-20 104 47 were be AUX eurjchem-20 104 48     SPACE eurjchem-20 104 49 evaluated evaluate VERB eurjchem-20 104 50     SPACE eurjchem-20 104 51 in in ADP eurjchem-20 104 52     SPACE eurjchem-20 104 53 mm mm NOUN eurjchem-20 104 54     SPACE eurjchem-20 104 55 using use VERB eurjchem-20 104 56     SPACE eurjchem-20 104 57 a a DET eurjchem-20 104 58     SPACE eurjchem-20 104 59 scale scale NOUN eurjchem-20 104 60 . . PUNCT eurjchem-20 104 61     SPACE eurjchem-20 105 1 the the DET eurjchem-20 105 2     SPACE eurjchem-20 105 3 experiment experiment NOUN eurjchem-20 105 4     SPACE eurjchem-20 105 5 was be AUX eurjchem-20 105 6     SPACE eurjchem-20 105 7 carried carry VERB eurjchem-20 105 8     SPACE eurjchem-20 105 9 out out ADP eurjchem-20 105 10     SPACE eurjchem-20 105 11 in in ADP eurjchem-20 105 12     SPACE eurjchem-20 105 13 triplicates triplicate NOUN eurjchem-20 105 14 . . PUNCT eurjchem-20 105 15       SPACE eurjchem-20 106 1 the the DET eurjchem-20 106 2     SPACE eurjchem-20 106 3 results result NOUN eurjchem-20 106 4     SPACE eurjchem-20 106 5 ( ( PUNCT eurjchem-20 106 6 table table NOUN eurjchem-20 106 7     SPACE eurjchem-20 106 8 1 1 NUM eurjchem-20 106 9 ) ) PUNCT eurjchem-20 106 10     SPACE eurjchem-20 106 11 were be AUX eurjchem-20 106 12     SPACE eurjchem-20 106 13 compared compare VERB eurjchem-20 106 14     SPACE eurjchem-20 106 15 with with ADP eurjchem-20 106 16     SPACE eurjchem-20 106 17 that that PRON eurjchem-20 106 18     SPACE eurjchem-20 106 19 of of ADP eurjchem-20 106 20     SPACE eurjchem-20 106 21 the the DET eurjchem-20 106 22     SPACE eurjchem-20 106 23 standard standard ADJ eurjchem-20 106 24     SPACE eurjchem-20 106 25 antibiotic antibiotic ADJ eurjchem-20 106 26     SPACE eurjchem-20 106 27 ampicillin ampicillin NOUN eurjchem-20 106 28     SPACE eurjchem-20 106 29 ( ( PUNCT eurjchem-20 106 30 100 100 NUM eurjchem-20 106 31     SPACE eurjchem-20 106 32 µg µg NOUN eurjchem-20 106 33 / / SYM eurjchem-20 106 34 ml ml NOUN eurjchem-20 106 35 ) ) PUNCT eurjchem-20 106 36 . . PUNCT eurjchem-20 106 37         SPACE eurjchem-20 107 1 2.3.2 2.3.2 NUM eurjchem-20 107 2 . . PUNCT eurjchem-20 107 3     SPACE eurjchem-20 107 4 antioxidant antioxidant ADJ eurjchem-20 107 5     SPACE eurjchem-20 107 6 activity activity NOUN eurjchem-20 107 7         SPACE eurjchem-20 107 8 the the DET eurjchem-20 107 9     SPACE eurjchem-20 107 10 antiradical antiradical ADJ eurjchem-20 107 11     SPACE eurjchem-20 107 12 activity activity NOUN eurjchem-20 107 13     SPACE eurjchem-20 107 14 of of ADP eurjchem-20 107 15     SPACE eurjchem-20 107 16 4a­l 4a­l NOUN eurjchem-20 107 17     SPACE eurjchem-20 107 18 was be AUX eurjchem-20 107 19     SPACE eurjchem-20 107 20 measured measure VERB eurjchem-20 107 21     SPACE eurjchem-20 107 22 in in ADP eurjchem-20 107 23     SPACE eurjchem-20 107 24 triplicate triplicate VERB eurjchem-20 107 25     SPACE eurjchem-20 107 26 using use VERB eurjchem-20 107 27     SPACE eurjchem-20 107 28 a a DET eurjchem-20 107 29     SPACE eurjchem-20 107 30 modified modify VERB eurjchem-20 107 31     SPACE eurjchem-20 107 32 burits burit NOUN eurjchem-20 107 33     SPACE eurjchem-20 107 34 and and CCONJ eurjchem-20 107 35     SPACE eurjchem-20 107 36 bucar bucar NOUN eurjchem-20 107 37     SPACE eurjchem-20 107 38 method method NOUN eurjchem-20 107 39     SPACE eurjchem-20 108 1 [ [ X eurjchem-20 108 2 13 13 NUM eurjchem-20 108 3 ] ] PUNCT eurjchem-20 108 4 . . PUNCT eurjchem-20 108 5     SPACE eurjchem-20 108 6 a a DET eurjchem-20 108 7     SPACE eurjchem-20 108 8 methanolic methanolic NOUN eurjchem-20 108 9     SPACE eurjchem-20 108 10 solution solution NOUN eurjchem-20 108 11     SPACE eurjchem-20 108 12 of of ADP eurjchem-20 108 13     SPACE eurjchem-20 108 14 dpph dpph PROPN eurjchem-20 108 15     SPACE eurjchem-20 108 16 ( ( PUNCT eurjchem-20 108 17 4 4 NUM eurjchem-20 108 18     SPACE eurjchem-20 108 19 ml ml NOUN eurjchem-20 108 20 , , PUNCT eurjchem-20 108 21     SPACE eurjchem-20 108 22 40 40 NUM eurjchem-20 108 23     SPACE eurjchem-20 108 24 ppm ppm NOUN eurjchem-20 108 25 ) ) PUNCT eurjchem-20 108 26     SPACE eurjchem-20 108 27 was be AUX eurjchem-20 108 28     SPACE eurjchem-20 108 29 added add VERB eurjchem-20 108 30     SPACE eurjchem-20 108 31 to to ADP eurjchem-20 108 32     SPACE eurjchem-20 108 33 1 1 NUM eurjchem-20 108 34     SPACE eurjchem-20 108 35 ml ml NOUN eurjchem-20 108 36     SPACE eurjchem-20 108 37 of of ADP eurjchem-20 108 38     SPACE eurjchem-20 108 39 the the DET eurjchem-20 108 40     SPACE eurjchem-20 108 41 antioxidant antioxidant NOUN eurjchem-20 108 42     SPACE eurjchem-20 108 43 solutions solution NOUN eurjchem-20 108 44     SPACE eurjchem-20 108 45 in in ADP eurjchem-20 108 46     SPACE eurjchem-20 108 47 0.1 0.1 NUM eurjchem-20 108 48     SPACE eurjchem-20 108 49 m m PROPN eurjchem-20 108 50     SPACE eurjchem-20 108 51 tris tris PROPN eurjchem-20 108 52 – – PUNCT eurjchem-20 108 53 hcl hcl NOUN eurjchem-20 108 54     SPACE eurjchem-20 108 55 buffer buffer NOUN eurjchem-20 108 56     SPACE eurjchem-20 108 57 ( ( PUNCT eurjchem-20 108 58 ph=7.1 ph=7.1 NOUN eurjchem-20 108 59 ) ) PUNCT eurjchem-20 108 60     SPACE eurjchem-20 108 61 at at ADP eurjchem-20 108 62     SPACE eurjchem-20 108 63 25 25 NUM eurjchem-20 108 64     SPACE eurjchem-20 108 65 ° ° NOUN eurjchem-20 108 66 c c NOUN eurjchem-20 108 67 , , PUNCT eurjchem-20 108 68     SPACE eurjchem-20 108 69 giving give VERB eurjchem-20 108 70     SPACE eurjchem-20 108 71 final final ADJ eurjchem-20 108 72     SPACE eurjchem-20 108 73 concentrations concentration NOUN eurjchem-20 108 74     SPACE eurjchem-20 108 75 of of ADP eurjchem-20 108 76     SPACE eurjchem-20 108 77 10 10 NUM eurjchem-20 108 78 , , PUNCT eurjchem-20 108 79     SPACE eurjchem-20 108 80 25 25 NUM eurjchem-20 108 81 , , PUNCT eurjchem-20 108 82     SPACE eurjchem-20 108 83 50 50 NUM eurjchem-20 108 84     SPACE eurjchem-20 108 85 and and CCONJ eurjchem-20 108 86     SPACE eurjchem-20 108 87 100 100 NUM eurjchem-20 108 88     SPACE eurjchem-20 108 89 μm μm NUM eurjchem-20 108 90 . . PUNCT eurjchem-20 108 91     SPACE eurjchem-20 108 92 the the DET eurjchem-20 108 93     SPACE eurjchem-20 108 94 absorbance absorbance NOUN eurjchem-20 108 95     SPACE eurjchem-20 108 96 read read NOUN eurjchem-20 108 97     SPACE eurjchem-20 108 98 at at ADP eurjchem-20 108 99     SPACE eurjchem-20 108 100 517 517 NUM eurjchem-20 108 101     SPACE eurjchem-20 108 102 nm nm VERB eurjchem-20 108 103     SPACE eurjchem-20 108 104 was be AUX eurjchem-20 108 105     SPACE eurjchem-20 108 106 measured measure VERB eurjchem-20 108 107     SPACE eurjchem-20 108 108 after after ADP eurjchem-20 108 109     SPACE eurjchem-20 108 110 60 60 NUM eurjchem-20 108 111     SPACE eurjchem-20 108 112 min min NOUN eurjchem-20 108 113     SPACE eurjchem-20 108 114 of of ADP eurjchem-20 108 115     SPACE eurjchem-20 108 116 the the DET eurjchem-20 108 117     SPACE eurjchem-20 108 118 reaction reaction NOUN eurjchem-20 108 119     SPACE eurjchem-20 108 120 in in ADP eurjchem-20 108 121     SPACE eurjchem-20 108 122 the the DET eurjchem-20 108 123     SPACE eurjchem-20 108 124 dark dark NOUN eurjchem-20 108 125     SPACE eurjchem-20 108 126 and and CCONJ eurjchem-20 108 127     SPACE eurjchem-20 108 128 compared compare VERB eurjchem-20 108 129     SPACE eurjchem-20 108 130 with with SCONJ eurjchem-20 108 131     SPACE eurjchem-20 108 132 the the DET eurjchem-20 108 133     SPACE eurjchem-20 108 134 control control NOUN eurjchem-20 108 135     SPACE eurjchem-20 108 136 prepared prepare VERB eurjchem-20 108 137     SPACE eurjchem-20 108 138 in in ADP eurjchem-20 108 139     SPACE eurjchem-20 108 140 a a DET eurjchem-20 108 141     SPACE eurjchem-20 108 142 similar similar ADJ eurjchem-20 108 143     SPACE eurjchem-20 108 144 way way NOUN eurjchem-20 108 145     SPACE eurjchem-20 108 146 without without ADP eurjchem-20 108 147     SPACE eurjchem-20 108 148 the the DET eurjchem-20 108 149     SPACE eurjchem-20 108 150 addition addition NOUN eurjchem-20 108 151     SPACE eurjchem-20 108 152 of of ADP eurjchem-20 108 153     SPACE eurjchem-20 108 154 the the DET eurjchem-20 108 155     SPACE eurjchem-20 108 156 antioxidants antioxidant NOUN eurjchem-20 108 157     SPACE eurjchem-20 108 158 ( ( PUNCT eurjchem-20 108 159 this this DET eurjchem-20 108 160     SPACE eurjchem-20 108 161 value value NOUN eurjchem-20 108 162     SPACE eurjchem-20 108 163 was be AUX eurjchem-20 108 164     SPACE eurjchem-20 108 165 assigned assign VERB eurjchem-20 108 166     SPACE eurjchem-20 108 167 arbitrarily arbitrarily ADV eurjchem-20 108 168     SPACE eurjchem-20 108 169 to to PART eurjchem-20 108 170     SPACE eurjchem-20 108 171 100 100 NUM eurjchem-20 108 172 % % NOUN eurjchem-20 108 173 ) ) PUNCT eurjchem-20 108 174 . . PUNCT eurjchem-20 108 175     SPACE eurjchem-20 109 1 a a DET eurjchem-20 109 2     SPACE eurjchem-20 109 3 100 100 NUM eurjchem-20 109 4     SPACE eurjchem-20 109 5 μm μm NUM eurjchem-20 109 6     SPACE eurjchem-20 109 7 solution solution NOUN eurjchem-20 109 8     SPACE eurjchem-20 109 9 of of ADP eurjchem-20 109 10     SPACE eurjchem-20 109 11 ascorbic ascorbic NOUN eurjchem-20 109 12     SPACE eurjchem-20 109 13 acid acid NOUN eurjchem-20 109 14     SPACE eurjchem-20 109 15 ( ( PUNCT eurjchem-20 109 16 a a DET eurjchem-20 109 17     SPACE eurjchem-20 109 18 strong strong ADJ eurjchem-20 109 19     SPACE eurjchem-20 109 20 and and CCONJ eurjchem-20 109 21     SPACE eurjchem-20 109 22 natural natural ADJ eurjchem-20 109 23     SPACE eurjchem-20 109 24 antioxidant antioxidant NOUN eurjchem-20 109 25     SPACE eurjchem-20 109 26 agent agent NOUN eurjchem-20 109 27 ) ) PUNCT eurjchem-20 109 28     SPACE eurjchem-20 109 29 was be AUX eurjchem-20 109 30     SPACE eurjchem-20 109 31 also also ADV eurjchem-20 109 32     SPACE eurjchem-20 109 33 tested test VERB eurjchem-20 109 34     SPACE eurjchem-20 109 35 as as ADP eurjchem-20 109 36     SPACE eurjchem-20 109 37 a a DET eurjchem-20 109 38     SPACE eurjchem-20 109 39 control control NOUN eurjchem-20 109 40     SPACE eurjchem-20 109 41 for for ADP eurjchem-20 109 42     SPACE eurjchem-20 109 43 the the DET eurjchem-20 109 44     SPACE eurjchem-20 109 45 reaction reaction NOUN eurjchem-20 109 46 . . PUNCT eurjchem-20 109 47     SPACE eurjchem-20 110 1 in in ADP eurjchem-20 110 2     SPACE eurjchem-20 110 3 this this DET eurjchem-20 110 4     SPACE eurjchem-20 110 5 case case NOUN eurjchem-20 110 6 , , PUNCT eurjchem-20 110 7     SPACE eurjchem-20 110 8 the the DET eurjchem-20 110 9     SPACE eurjchem-20 110 10 violet violet NOUN eurjchem-20 110 11     SPACE eurjchem-20 110 12 color color NOUN eurjchem-20 110 13     SPACE eurjchem-20 110 14 of of ADP eurjchem-20 110 15     SPACE eurjchem-20 110 16 dpph dpph PROPN eurjchem-20 110 17     SPACE eurjchem-20 110 18 disappeared disappear VERB eurjchem-20 110 19     SPACE eurjchem-20 110 20 immediately immediately ADV eurjchem-20 110 21 . . PUNCT eurjchem-20 110 22     SPACE eurjchem-20 111 1 it it PRON eurjchem-20 111 2     SPACE eurjchem-20 111 3 is be AUX eurjchem-20 111 4     SPACE eurjchem-20 111 5 confirmed confirm VERB eurjchem-20 111 6     SPACE eurjchem-20 111 7 that that SCONJ eurjchem-20 111 8     SPACE eurjchem-20 111 9 the the DET eurjchem-20 111 10     SPACE eurjchem-20 111 11 test test NOUN eurjchem-20 111 12     SPACE eurjchem-20 111 13 compounds compound NOUN eurjchem-20 111 14     SPACE eurjchem-20 111 15 showed show VERB eurjchem-20 111 16     SPACE eurjchem-20 111 17 better well ADJ eurjchem-20 111 18     SPACE eurjchem-20 111 19 antioxidant antioxidant NOUN eurjchem-20 111 20     SPACE eurjchem-20 111 21 activity activity NOUN eurjchem-20 111 22     SPACE eurjchem-20 111 23 when when SCONJ eurjchem-20 111 24     SPACE eurjchem-20 111 25 compared compare VERB eurjchem-20 111 26     SPACE eurjchem-20 111 27 to to ADP eurjchem-20 111 28     SPACE eurjchem-20 111 29 the the DET eurjchem-20 111 30     SPACE eurjchem-20 111 31 parent parent NOUN eurjchem-20 111 32     SPACE eurjchem-20 111 33 drug drug NOUN eurjchem-20 111 34     SPACE eurjchem-20 111 35 stavudine stavudine NOUN eurjchem-20 111 36     SPACE eurjchem-20 111 37 and and CCONJ eurjchem-20 111 38     SPACE eurjchem-20 111 39 moderate moderate ADJ eurjchem-20 111 40     SPACE eurjchem-20 111 41 activity activity NOUN eurjchem-20 111 42     SPACE eurjchem-20 111 43 when when SCONJ eurjchem-20 111 44     SPACE eurjchem-20 111 45 compared compare VERB eurjchem-20 111 46     SPACE eurjchem-20 111 47 with with ADP eurjchem-20 111 48     SPACE eurjchem-20 111 49 that that PRON eurjchem-20 111 50     SPACE eurjchem-20 111 51 of of ADP eurjchem-20 111 52     SPACE eurjchem-20 111 53 vitamin vitamin NOUN eurjchem-20 111 54     SPACE eurjchem-20 111 55 c c NOUN eurjchem-20 111 56     SPACE eurjchem-20 111 57 ( ( PUNCT eurjchem-20 111 58 table table NOUN eurjchem-20 111 59     SPACE eurjchem-20 111 60 2 2 NUM eurjchem-20 111 61 ) ) PUNCT eurjchem-20 111 62 . . PUNCT eurjchem-20 111 63         SPACE eurjchem-20 111 64 antioxidant antioxidant ADJ eurjchem-20 111 65     SPACE eurjchem-20 111 66 activity activity NOUN eurjchem-20 111 67     SPACE eurjchem-20 111 68 ( ( PUNCT eurjchem-20 111 69 % % NOUN eurjchem-20 111 70 ) ) PUNCT eurjchem-20 111 71     SPACE eurjchem-20 112 1 = = NOUN eurjchem-20 112 2     SPACE eurjchem-20 112 3 [ [ X eurjchem-20 112 4 ( ( PUNCT eurjchem-20 112 5 a517control a517control NOUN eurjchem-20 112 6     SPACE eurjchem-20 112 7 ‐ ‐ NOUN eurjchem-20 112 8     SPACE eurjchem-20 112 9 a517sample a517sample NOUN eurjchem-20 112 10 ) ) PUNCT eurjchem-20 112 11     SPACE eurjchem-20 112 12 /a517control /a517control NOUN eurjchem-20 112 13 ] ] X eurjchem-20 112 14     SPACE eurjchem-20 112 15 x x NOUN eurjchem-20 112 16     SPACE eurjchem-20 112 17 100 100 NUM eurjchem-20 112 18       SPACE eurjchem-20 112 19 ( ( PUNCT eurjchem-20 112 20 1 1 NUM eurjchem-20 112 21 ) ) PUNCT eurjchem-20 112 22         SPACE eurjchem-20 112 23 table table NOUN eurjchem-20 112 24     SPACE eurjchem-20 112 25 2 2 NUM eurjchem-20 112 26 . . PUNCT eurjchem-20 112 27     SPACE eurjchem-20 112 28 dpph dpph PROPN eurjchem-20 112 29     SPACE eurjchem-20 112 30 radical radical ADJ eurjchem-20 112 31     SPACE eurjchem-20 112 32 scavenging scavenge VERB eurjchem-20 112 33     SPACE eurjchem-20 112 34 activity activity NOUN eurjchem-20 112 35     SPACE eurjchem-20 112 36 of of ADP eurjchem-20 112 37     SPACE eurjchem-20 112 38 ( ( PUNCT eurjchem-20 112 39 4a­l 4a­l PROPN eurjchem-20 112 40 ) ) PUNCT eurjchem-20 112 41 . . PUNCT eurjchem-20 112 42     SPACE eurjchem-20 112 43 compounds compound VERB eurjchem-20 112 44     SPACE eurjchem-20 112 45 ic50 ic50 PROPN eurjchem-20 112 46     SPACE eurjchem-20 112 47 / / SYM eurjchem-20 112 48     SPACE eurjchem-20 112 49 dpphvalues(μg dpphvalues(μg NOUN eurjchem-20 112 50 / / SYM eurjchem-20 112 51 ml ml NOUN eurjchem-20 112 52 ) ) PUNCT eurjchem-20 112 53     SPACE eurjchem-20 112 54 4a 4a NOUN eurjchem-20 112 55     SPACE eurjchem-20 112 56 150.66 150.66 NUM eurjchem-20 112 57     SPACE eurjchem-20 112 58 ± ± NOUN eurjchem-20 112 59     SPACE eurjchem-20 112 60 6.95 6.95 NUM eurjchem-20 112 61     SPACE eurjchem-20 112 62 4b 4b NOUN eurjchem-20 112 63     SPACE eurjchem-20 112 64 187.56 187.56 NUM eurjchem-20 112 65     SPACE eurjchem-20 112 66 ± ± NOUN eurjchem-20 112 67     SPACE eurjchem-20 112 68 9.31 9.31 NUM eurjchem-20 112 69     SPACE eurjchem-20 112 70 4c 4c NOUN eurjchem-20 112 71     SPACE eurjchem-20 112 72 149.33 149.33 NUM eurjchem-20 112 73     SPACE eurjchem-20 112 74 ± ± NOUN eurjchem-20 112 75     SPACE eurjchem-20 112 76 4.43 4.43 NUM eurjchem-20 112 77     SPACE eurjchem-20 112 78 4d 4d NOUN eurjchem-20 112 79     SPACE eurjchem-20 112 80 122.79 122.79 NUM eurjchem-20 112 81     SPACE eurjchem-20 112 82 ± ± NOUN eurjchem-20 112 83     SPACE eurjchem-20 112 84 2.51 2.51 NUM eurjchem-20 112 85     SPACE eurjchem-20 112 86 4e 4e NOUN eurjchem-20 112 87     SPACE eurjchem-20 112 88 110.39 110.39 NUM eurjchem-20 112 89     SPACE eurjchem-20 112 90 ± ± NOUN eurjchem-20 112 91     SPACE eurjchem-20 112 92 7.55 7.55 NUM eurjchem-20 112 93     SPACE eurjchem-20 112 94 4f 4f NUM eurjchem-20 112 95     SPACE eurjchem-20 112 96 119.06± 119.06± NOUN eurjchem-20 112 97     SPACE eurjchem-20 112 98 0.84 0.84 NUM eurjchem-20 112 99     SPACE eurjchem-20 112 100 4 4 NUM eurjchem-20 112 101 g g NOUN eurjchem-20 112 102     SPACE eurjchem-20 112 103 162.33 162.33 NUM eurjchem-20 112 104     SPACE eurjchem-20 112 105 ± ± NOUN eurjchem-20 112 106     SPACE eurjchem-20 112 107 5.45 5.45 NUM eurjchem-20 112 108     SPACE eurjchem-20 112 109 4h 4h NUM eurjchem-20 112 110     SPACE eurjchem-20 112 111 127.49 127.49 NUM eurjchem-20 112 112     SPACE eurjchem-20 112 113 ± ± NOUN eurjchem-20 112 114     SPACE eurjchem-20 112 115 6.47 6.47 NUM eurjchem-20 112 116     SPACE eurjchem-20 112 117 4i 4i NOUN eurjchem-20 112 118     SPACE eurjchem-20 112 119 112.94 112.94 NUM eurjchem-20 112 120     SPACE eurjchem-20 112 121 ± ± NOUN eurjchem-20 112 122     SPACE eurjchem-20 112 123 4.73 4.73 NUM eurjchem-20 112 124     SPACE eurjchem-20 112 125 4j 4j NOUN eurjchem-20 112 126     SPACE eurjchem-20 112 127 132.67 132.67 NUM eurjchem-20 112 128     SPACE eurjchem-20 112 129 ± ± NOUN eurjchem-20 112 130     SPACE eurjchem-20 112 131 7.76 7.76 NUM eurjchem-20 112 132     SPACE eurjchem-20 112 133 4k 4k NOUN eurjchem-20 112 134     SPACE eurjchem-20 112 135 157.56 157.56 NUM eurjchem-20 112 136     SPACE eurjchem-20 112 137 ± ± NOUN eurjchem-20 112 138     SPACE eurjchem-20 112 139 5.28 5.28 NUM eurjchem-20 112 140     SPACE eurjchem-20 112 141 4l 4l NOUN eurjchem-20 112 142     SPACE eurjchem-20 112 143 162.71 162.71 NUM eurjchem-20 112 144     SPACE eurjchem-20 112 145 ± ± NOUN eurjchem-20 112 146     SPACE eurjchem-20 112 147 3.37 3.37 NUM eurjchem-20 112 148     SPACE eurjchem-20 112 149 stavudine stavudine ADJ eurjchem-20 112 150     SPACE eurjchem-20 112 151 244.82 244.82 NUM eurjchem-20 112 152     SPACE eurjchem-20 112 153 ± ± NOUN eurjchem-20 112 154     SPACE eurjchem-20 112 155 6.21 6.21 NUM eurjchem-20 112 156     SPACE eurjchem-20 112 157 vitamin vitamin NOUN eurjchem-20 112 158     SPACE eurjchem-20 112 159 c c NOUN eurjchem-20 112 160     SPACE eurjchem-20 112 161 71.30 71.30 NUM eurjchem-20 112 162     SPACE eurjchem-20 112 163 ± ± NOUN eurjchem-20 112 164     SPACE eurjchem-20 112 165 1.66 1.66 NUM eurjchem-20 112 166         SPACE eurjchem-20 112 167 3 3 NUM eurjchem-20 112 168 . . PUNCT eurjchem-20 112 169     SPACE eurjchem-20 112 170 results result VERB eurjchem-20 112 171     SPACE eurjchem-20 112 172 and and CCONJ eurjchem-20 112 173     SPACE eurjchem-20 112 174 discussion discussion NOUN eurjchem-20 112 175           SPACE eurjchem-20 112 176 the the DET eurjchem-20 112 177     SPACE eurjchem-20 112 178 synthesis synthesis NOUN eurjchem-20 112 179     SPACE eurjchem-20 112 180 of of ADP eurjchem-20 112 181     SPACE eurjchem-20 112 182 the the DET eurjchem-20 112 183     SPACE eurjchem-20 112 184 phosphorylated phosphorylate VERB eurjchem-20 112 185     SPACE eurjchem-20 112 186 derivatives derivative NOUN eurjchem-20 112 187     SPACE eurjchem-20 112 188 of of ADP eurjchem-20 112 189     SPACE eurjchem-20 112 190 stavudine stavudine ADJ eurjchem-20 112 191     SPACE eurjchem-20 112 192 4a­l 4a­l NOUN eurjchem-20 112 193     SPACE eurjchem-20 112 194 is be AUX eurjchem-20 112 195     SPACE eurjchem-20 112 196 depicted depict VERB eurjchem-20 112 197     SPACE eurjchem-20 112 198 in in ADP eurjchem-20 112 199     SPACE eurjchem-20 112 200 scheme scheme NOUN eurjchem-20 112 201     SPACE eurjchem-20 112 202 1 1 NUM eurjchem-20 112 203 . . PUNCT eurjchem-20 112 204     SPACE eurjchem-20 112 205 cyclic cyclic ADJ eurjchem-20 112 206     SPACE eurjchem-20 112 207 amines amine NOUN eurjchem-20 112 208     SPACE eurjchem-20 112 209 and and CCONJ eurjchem-20 112 210     SPACE eurjchem-20 112 211 amino amino NOUN eurjchem-20 112 212     SPACE eurjchem-20 112 213 acid acid NOUN eurjchem-20 112 214     SPACE eurjchem-20 112 215 esters ester NOUN eurjchem-20 112 216     SPACE eurjchem-20 112 217 were be AUX eurjchem-20 112 218     SPACE eurjchem-20 112 219 reacted react VERB eurjchem-20 112 220     SPACE eurjchem-20 112 221 with with ADP eurjchem-20 112 222     SPACE eurjchem-20 112 223 bis(2‐chloroethyl bis(2‐chloroethyl NOUN eurjchem-20 112 224 ) ) PUNCT eurjchem-20 112 225     SPACE eurjchem-20 112 226 phosphoramidic phosphoramidic ADJ eurjchem-20 112 227     SPACE eurjchem-20 112 228 dichloride dichloride NOUN eurjchem-20 112 229     SPACE eurjchem-20 112 230 and and CCONJ eurjchem-20 112 231     SPACE eurjchem-20 112 232 4‐nitro 4‐nitro ADJ eurjchem-20 112 233     SPACE eurjchem-20 112 234 phenyl phenyl NOUN eurjchem-20 112 235     SPACE eurjchem-20 112 236 phosphoro phosphoro NOUN eurjchem-20 112 237     SPACE eurjchem-20 112 238 dichloridate dichloridate ADJ eurjchem-20 112 239     SPACE eurjchem-20 112 240 at at ADP eurjchem-20 112 241     SPACE eurjchem-20 112 242 ‐10 ‐10 NOUN eurjchem-20 112 243     SPACE eurjchem-20 112 244 ° ° NOUN eurjchem-20 112 245 c c NOUN eurjchem-20 112 246     SPACE eurjchem-20 112 247 ( ( PUNCT eurjchem-20 112 248 scheme scheme NOUN eurjchem-20 112 249     SPACE eurjchem-20 112 250 1 1 NUM eurjchem-20 112 251 ) ) PUNCT eurjchem-20 112 252 , , PUNCT eurjchem-20 112 253     SPACE eurjchem-20 112 254 in in ADP eurjchem-20 112 255     SPACE eurjchem-20 112 256 the the DET eurjchem-20 112 257     SPACE eurjchem-20 112 258 presence presence NOUN eurjchem-20 112 259     SPACE eurjchem-20 112 260 of of ADP eurjchem-20 112 261     SPACE eurjchem-20 112 262 tea tea NOUN eurjchem-20 112 263     SPACE eurjchem-20 112 264 in in ADP eurjchem-20 112 265     SPACE eurjchem-20 112 266 thf thf NOUN eurjchem-20 112 267 . . PUNCT eurjchem-20 112 268     SPACE eurjchem-20 113 1 the the DET eurjchem-20 113 2     SPACE eurjchem-20 113 3 progress progress NOUN eurjchem-20 113 4     SPACE eurjchem-20 113 5 of of ADP eurjchem-20 113 6     SPACE eurjchem-20 113 7 the the DET eurjchem-20 113 8     SPACE eurjchem-20 113 9 reaction reaction NOUN eurjchem-20 113 10     SPACE eurjchem-20 113 11 was be AUX eurjchem-20 113 12     SPACE eurjchem-20 113 13 monitored monitor VERB eurjchem-20 113 14     SPACE eurjchem-20 113 15 by by ADP eurjchem-20 113 16     SPACE eurjchem-20 113 17 tlc tlc NOUN eurjchem-20 113 18 . . PUNCT eurjchem-20 113 19     SPACE eurjchem-20 113 20 after after ADP eurjchem-20 113 21     SPACE eurjchem-20 113 22 completion completion NOUN eurjchem-20 113 23     SPACE eurjchem-20 113 24 of of ADP eurjchem-20 113 25     SPACE eurjchem-20 113 26 the the DET eurjchem-20 113 27     SPACE eurjchem-20 113 28 reaction reaction NOUN eurjchem-20 113 29     SPACE eurjchem-20 113 30 in in ADP eurjchem-20 113 31     SPACE eurjchem-20 113 32 2 2 NUM eurjchem-20 113 33     SPACE eurjchem-20 113 34 h h NOUN eurjchem-20 113 35 , , PUNCT eurjchem-20 113 36     SPACE eurjchem-20 113 37 a a DET eurjchem-20 113 38     SPACE eurjchem-20 113 39 solution solution NOUN eurjchem-20 113 40     SPACE eurjchem-20 113 41 of of ADP eurjchem-20 113 42     SPACE eurjchem-20 113 43 stavudine stavudine NOUN eurjchem-20 113 44     SPACE eurjchem-20 113 45 and and CCONJ eurjchem-20 113 46     SPACE eurjchem-20 113 47 tea tea NOUN eurjchem-20 113 48     SPACE eurjchem-20 113 49 in in ADP eurjchem-20 113 50     SPACE eurjchem-20 113 51 pyridine pyridine NOUN eurjchem-20 113 52     SPACE eurjchem-20 113 53 was be AUX eurjchem-20 113 54     SPACE eurjchem-20 113 55 added add VERB eurjchem-20 113 56     SPACE eurjchem-20 113 57 to to ADP eurjchem-20 113 58     SPACE eurjchem-20 113 59 the the DET eurjchem-20 113 60     SPACE eurjchem-20 113 61 reaction reaction NOUN eurjchem-20 113 62     SPACE eurjchem-20 113 63 mixture mixture NOUN eurjchem-20 113 64     SPACE eurjchem-20 113 65 at at ADP eurjchem-20 113 66     SPACE eurjchem-20 113 67 10 10 NUM eurjchem-20 113 68     SPACE eurjchem-20 113 69 ° ° NOUN eurjchem-20 113 70 c c NOUN eurjchem-20 113 71     SPACE eurjchem-20 113 72 and and CCONJ eurjchem-20 113 73     SPACE eurjchem-20 113 74 the the DET eurjchem-20 113 75     SPACE eurjchem-20 113 76 mixture mixture NOUN eurjchem-20 113 77     SPACE eurjchem-20 113 78 was be AUX eurjchem-20 113 79     SPACE eurjchem-20 113 80 stirred stir VERB eurjchem-20 113 81     SPACE eurjchem-20 113 82 for for ADP eurjchem-20 113 83     SPACE eurjchem-20 113 84 10 10 NUM eurjchem-20 113 85     SPACE eurjchem-20 113 86 h h NOUN eurjchem-20 113 87     SPACE eurjchem-20 113 88 at at ADP eurjchem-20 113 89     SPACE eurjchem-20 113 90 rt rt PROPN eurjchem-20 113 91 . . PUNCT eurjchem-20 113 92     SPACE eurjchem-20 113 93 the the DET eurjchem-20 113 94     SPACE eurjchem-20 113 95 reaction reaction NOUN eurjchem-20 113 96     SPACE eurjchem-20 113 97 was be AUX eurjchem-20 113 98     SPACE eurjchem-20 113 99 completed complete VERB eurjchem-20 113 100     SPACE eurjchem-20 113 101 as as SCONJ eurjchem-20 113 102     SPACE eurjchem-20 113 103 indicated indicate VERB eurjchem-20 113 104     SPACE eurjchem-20 113 105 by by ADP eurjchem-20 113 106     SPACE eurjchem-20 113 107 tlc tlc NOUN eurjchem-20 113 108 , , PUNCT eurjchem-20 113 109     SPACE eurjchem-20 113 110 ( ( PUNCT eurjchem-20 113 111 ethylacetate ethylacetate VERB eurjchem-20 113 112 : : PUNCT eurjchem-20 113 113 hexane hexane NOUN eurjchem-20 113 114 , , PUNCT eurjchem-20 113 115     SPACE eurjchem-20 113 116 9:1 9:1 NUM eurjchem-20 113 117 ) ) PUNCT eurjchem-20 113 118 , , PUNCT eurjchem-20 113 119     SPACE eurjchem-20 113 120 tea tea NOUN eurjchem-20 113 121     SPACE eurjchem-20 113 122 hydrochloride hydrochloride NOUN eurjchem-20 113 123     SPACE eurjchem-20 113 124 was be AUX eurjchem-20 113 125     SPACE eurjchem-20 113 126 removed remove VERB eurjchem-20 113 127     SPACE eurjchem-20 113 128 by by ADP eurjchem-20 113 129     SPACE eurjchem-20 113 130 filtration filtration NOUN eurjchem-20 113 131     SPACE eurjchem-20 113 132 and and CCONJ eurjchem-20 113 133     SPACE eurjchem-20 113 134 the the DET eurjchem-20 113 135     SPACE eurjchem-20 113 136 solvent solvent NOUN eurjchem-20 113 137       SPACE eurjchem-20 113 138 from from ADP eurjchem-20 113 139     SPACE eurjchem-20 113 140 the the DET eurjchem-20 113 141     SPACE eurjchem-20 113 142 filtrate filtrate NOUN eurjchem-20 113 143     SPACE eurjchem-20 113 144 was be AUX eurjchem-20 113 145     SPACE eurjchem-20 113 146 removed remove VERB eurjchem-20 113 147     SPACE eurjchem-20 113 148 in in ADP eurjchem-20 113 149     SPACE eurjchem-20 113 150 vacuum vacuum NOUN eurjchem-20 113 151 . . PUNCT eurjchem-20 113 152     SPACE eurjchem-20 114 1 the the DET eurjchem-20 114 2     SPACE eurjchem-20 114 3 residue residue NOUN eurjchem-20 114 4     SPACE eurjchem-20 114 5 was be AUX eurjchem-20 114 6     SPACE eurjchem-20 114 7 column column NOUN eurjchem-20 114 8     SPACE eurjchem-20 114 9 chromatographed chromatographe VERB eurjchem-20 114 10     SPACE eurjchem-20 114 11 on on ADP eurjchem-20 114 12     SPACE eurjchem-20 114 13 silica silica NOUN eurjchem-20 114 14     SPACE eurjchem-20 114 15 and and CCONJ eurjchem-20 114 16     SPACE eurjchem-20 114 17 eluted elute VERB eurjchem-20 114 18     SPACE eurjchem-20 114 19 with with ADP eurjchem-20 114 20     SPACE eurjchem-20 114 21 1 1 NUM eurjchem-20 114 22 % % NOUN eurjchem-20 114 23     SPACE eurjchem-20 114 24 methanol methanol NOUN eurjchem-20 114 25     SPACE eurjchem-20 114 26 in in ADP eurjchem-20 114 27     SPACE eurjchem-20 114 28 chloroform chloroform NOUN eurjchem-20 114 29 . . PUNCT eurjchem-20 114 30     SPACE eurjchem-20 115 1 all all PRON eurjchem-20 115 2     SPACE eurjchem-20 115 3 the the DET eurjchem-20 115 4     SPACE eurjchem-20 115 5 compounds compound NOUN eurjchem-20 115 6     SPACE eurjchem-20 115 7 4a­l 4a­l PROPN eurjchem-20 115 8     SPACE eurjchem-20 115 9 exhibited exhibit VERB eurjchem-20 115 10     SPACE eurjchem-20 115 11 characteristic characteristic NOUN eurjchem-20 115 12     SPACE eurjchem-20 115 13 infrared infrare VERB eurjchem-20 115 14     SPACE eurjchem-20 115 15 absorption absorption NOUN eurjchem-20 115 16     SPACE eurjchem-20 115 17 bands band NOUN eurjchem-20 115 18     SPACE eurjchem-20 115 19 for for ADP eurjchem-20 115 20     SPACE eurjchem-20 115 21 p p PROPN eurjchem-20 115 22 = = PROPN eurjchem-20 115 23 o o NOUN eurjchem-20 115 24 , , PUNCT eurjchem-20 115 25     SPACE eurjchem-20 115 26 c c NOUN eurjchem-20 115 27 = = VERB eurjchem-20 115 28 o o NOUN eurjchem-20 115 29     SPACE eurjchem-20 115 30 and and CCONJ eurjchem-20 115 31     SPACE eurjchem-20 115 32 nh nh NOUN eurjchem-20 115 33     SPACE eurjchem-20 115 34 in in ADP eurjchem-20 115 35     SPACE eurjchem-20 115 36 the the DET eurjchem-20 115 37     SPACE eurjchem-20 115 38 regions region NOUN eurjchem-20 115 39     SPACE eurjchem-20 115 40 1218‐1236 1218‐1236 NUM eurjchem-20 115 41 , , PUNCT eurjchem-20 115 42     SPACE eurjchem-20 115 43 1683‐1731 1683‐1731 NUM eurjchem-20 115 44     SPACE eurjchem-20 115 45 and and CCONJ eurjchem-20 115 46     SPACE eurjchem-20 115 47 3394‐3375 3394‐3375 NOUN eurjchem-20 115 48     SPACE eurjchem-20 115 49 cm‐1 cm‐1 NOUN eurjchem-20 115 50 , , PUNCT eurjchem-20 115 51     SPACE eurjchem-20 115 52 respectively respectively ADV eurjchem-20 115 53     SPACE eurjchem-20 116 1 [ [ X eurjchem-20 116 2 14 14 NUM eurjchem-20 116 3 ] ] PUNCT eurjchem-20 116 4 . . PUNCT eurjchem-20 116 5     SPACE eurjchem-20 117 1 rao rao PROPN eurjchem-20 117 2     SPACE eurjchem-20 117 3 et et PROPN eurjchem-20 117 4     SPACE eurjchem-20 117 5 al al PROPN eurjchem-20 117 6 . . PROPN eurjchem-20 117 7     SPACE eurjchem-20 117 8 / / SYM eurjchem-20 117 9     SPACE eurjchem-20 117 10 european european ADJ eurjchem-20 117 11     SPACE eurjchem-20 117 12 journal journal NOUN eurjchem-20 117 13     SPACE eurjchem-20 117 14 of of ADP eurjchem-20 117 15     SPACE eurjchem-20 117 16 chemistry chemistry NOUN eurjchem-20 117 17     SPACE eurjchem-20 117 18 1 1 NUM eurjchem-20 117 19     SPACE eurjchem-20 117 20 ( ( PUNCT eurjchem-20 117 21 4 4 NUM eurjchem-20 117 22 ) ) PUNCT eurjchem-20 117 23     SPACE eurjchem-20 117 24 ( ( PUNCT eurjchem-20 117 25 2010 2010 NUM eurjchem-20 117 26 ) ) PUNCT eurjchem-20 117 27     SPACE eurjchem-20 118 1 297­301 297­301 NUM eurjchem-20 118 2     SPACE eurjchem-20 118 3 301 301 NUM eurjchem-20 118 4     SPACE eurjchem-20 118 5 the the DET eurjchem-20 118 6     SPACE eurjchem-20 118 7 chemical chemical NOUN eurjchem-20 118 8     SPACE eurjchem-20 118 9 shifts shift NOUN eurjchem-20 118 10     SPACE eurjchem-20 118 11 of of ADP eurjchem-20 118 12     SPACE eurjchem-20 118 13 the the DET eurjchem-20 118 14     SPACE eurjchem-20 118 15 nh nh NOUN eurjchem-20 118 16     SPACE eurjchem-20 118 17 protons proton NOUN eurjchem-20 118 18     SPACE eurjchem-20 118 19 in in ADP eurjchem-20 118 20     SPACE eurjchem-20 118 21 thymine thymine NOUN eurjchem-20 118 22     SPACE eurjchem-20 118 23 ring ring NOUN eurjchem-20 118 24     SPACE eurjchem-20 118 25 were be AUX eurjchem-20 118 26     SPACE eurjchem-20 118 27 observed observe VERB eurjchem-20 118 28     SPACE eurjchem-20 118 29 as as ADP eurjchem-20 118 30     SPACE eurjchem-20 118 31 a a DET eurjchem-20 118 32     SPACE eurjchem-20 118 33 singlet singlet NOUN eurjchem-20 118 34     SPACE eurjchem-20 118 35 in in ADP eurjchem-20 118 36     SPACE eurjchem-20 118 37 the the DET eurjchem-20 118 38     SPACE eurjchem-20 118 39 region region NOUN eurjchem-20 118 40     SPACE eurjchem-20 118 41 d d NUM eurjchem-20 118 42     SPACE eurjchem-20 118 43 8.1‐11.2 8.1‐11.2 NOUN eurjchem-20 118 44 . . PUNCT eurjchem-20 118 45     SPACE eurjchem-20 119 1 [ [ X eurjchem-20 119 2 15‐16 15‐16 NUM eurjchem-20 119 3 ] ] X eurjchem-20 119 4 . . PUNCT eurjchem-20 119 5     SPACE eurjchem-20 119 6 the the DET eurjchem-20 119 7     SPACE eurjchem-20 119 8 h‐6 h‐6 NOUN eurjchem-20 119 9 ' ' NUM eurjchem-20 119 10     SPACE eurjchem-20 119 11 proton proton NOUN eurjchem-20 119 12     SPACE eurjchem-20 119 13 signal signal NOUN eurjchem-20 119 14     SPACE eurjchem-20 119 15 appeared appear VERB eurjchem-20 119 16     SPACE eurjchem-20 119 17 as as ADP eurjchem-20 119 18     SPACE eurjchem-20 119 19 a a DET eurjchem-20 119 20     SPACE eurjchem-20 119 21 doublet doublet NOUN eurjchem-20 119 22     SPACE eurjchem-20 119 23 in in ADP eurjchem-20 119 24     SPACE eurjchem-20 119 25 the the DET eurjchem-20 119 26     SPACE eurjchem-20 119 27 region region NOUN eurjchem-20 119 28     SPACE eurjchem-20 119 29 7.43‐7.7 7.43‐7.7 NUM eurjchem-20 119 30     SPACE eurjchem-20 119 31 ppm ppm NOUN eurjchem-20 119 32     SPACE eurjchem-20 119 33 [ [ X eurjchem-20 119 34 17 17 NUM eurjchem-20 119 35 ] ] PUNCT eurjchem-20 119 36 . . PUNCT eurjchem-20 119 37     SPACE eurjchem-20 119 38 in in ADP eurjchem-20 119 39     SPACE eurjchem-20 119 40 13c 13c NOUN eurjchem-20 119 41     SPACE eurjchem-20 119 42 nmr nmr NOUN eurjchem-20 119 43     SPACE eurjchem-20 119 44 the the DET eurjchem-20 119 45     SPACE eurjchem-20 119 46 chemical chemical NOUN eurjchem-20 119 47     SPACE eurjchem-20 119 48 shifts shift NOUN eurjchem-20 119 49     SPACE eurjchem-20 119 50 of of ADP eurjchem-20 119 51     SPACE eurjchem-20 119 52 the the DET eurjchem-20 119 53     SPACE eurjchem-20 119 54 carbonyl carbonyl NOUN eurjchem-20 119 55     SPACE eurjchem-20 119 56 carbon carbon NOUN eurjchem-20 119 57     SPACE eurjchem-20 119 58 of of ADP eurjchem-20 119 59     SPACE eurjchem-20 119 60 thymine thymine NOUN eurjchem-20 119 61     SPACE eurjchem-20 119 62 ring ring NOUN eurjchem-20 119 63     SPACE eurjchem-20 119 64 resonated resonate VERB eurjchem-20 119 65     SPACE eurjchem-20 119 66 at at ADP eurjchem-20 119 67         SPACE eurjchem-20 119 68   NUM eurjchem-20 119 69         SPACE eurjchem-20 119 70 164.5‐150.2 164.5‐150.2 NUM eurjchem-20 119 71     SPACE eurjchem-20 120 1 [ [ X eurjchem-20 120 2 17 17 NUM eurjchem-20 120 3 ] ] PUNCT eurjchem-20 120 4 . . PUNCT eurjchem-20 120 5     SPACE eurjchem-20 120 6 the the DET eurjchem-20 120 7     SPACE eurjchem-20 120 8 31p 31p NOUN eurjchem-20 120 9     SPACE eurjchem-20 120 10 nmr nmr NOUN eurjchem-20 120 11     SPACE eurjchem-20 120 12 chemical chemical NOUN eurjchem-20 120 13     SPACE eurjchem-20 120 14 shifts shift NOUN eurjchem-20 120 15     SPACE eurjchem-20 120 16 appeared appear VERB eurjchem-20 120 17     SPACE eurjchem-20 120 18 in in ADP eurjchem-20 120 19     SPACE eurjchem-20 120 20 the the DET eurjchem-20 120 21     SPACE eurjchem-20 120 22 region region NOUN eurjchem-20 120 23     SPACE eurjchem-20 120 24 ‐1.24 ‐1.24 NOUN eurjchem-20 120 25     SPACE eurjchem-20 120 26 to to ADP eurjchem-20 120 27     SPACE eurjchem-20 120 28 7.85 7.85 NUM eurjchem-20 120 29     SPACE eurjchem-20 120 30 ppm ppm NOUN eurjchem-20 120 31     SPACE eurjchem-20 121 1 [ [ X eurjchem-20 121 2 18 18 NUM eurjchem-20 121 3 ] ] PUNCT eurjchem-20 121 4 . . PUNCT eurjchem-20 121 5     SPACE eurjchem-20 122 1 the the DET eurjchem-20 122 2     SPACE eurjchem-20 122 3 compounds compound NOUN eurjchem-20 122 4     SPACE eurjchem-20 122 5 4a 4a NOUN eurjchem-20 122 6 , , PUNCT eurjchem-20 122 7     SPACE eurjchem-20 122 8 4d 4d NUM eurjchem-20 122 9 , , PUNCT eurjchem-20 122 10     SPACE eurjchem-20 122 11 4e 4e NOUN eurjchem-20 122 12 , , PUNCT eurjchem-20 122 13     SPACE eurjchem-20 122 14 4h 4h NOUN eurjchem-20 122 15     SPACE eurjchem-20 122 16 and and CCONJ eurjchem-20 122 17     SPACE eurjchem-20 122 18 4i 4i NOUN eurjchem-20 122 19     SPACE eurjchem-20 122 20 exhibited exhibit VERB eurjchem-20 122 21     SPACE eurjchem-20 122 22 molecular molecular ADJ eurjchem-20 122 23     SPACE eurjchem-20 122 24 ion ion NOUN eurjchem-20 122 25     SPACE eurjchem-20 122 26 peaks peak NOUN eurjchem-20 122 27     SPACE eurjchem-20 122 28 with with ADP eurjchem-20 122 29     SPACE eurjchem-20 122 30 moderate moderate ADJ eurjchem-20 122 31     SPACE eurjchem-20 122 32 intensity intensity NOUN eurjchem-20 122 33     SPACE eurjchem-20 122 34 in in ADP eurjchem-20 122 35     SPACE eurjchem-20 122 36 their their PRON eurjchem-20 122 37     SPACE eurjchem-20 122 38 gc gc PROPN eurjchem-20 122 39     SPACE eurjchem-20 122 40 mass mass PROPN eurjchem-20 122 41     SPACE eurjchem-20 122 42 spectra spectra NOUN eurjchem-20 122 43 . . PUNCT eurjchem-20 122 44     SPACE eurjchem-20 122 45 the the DET eurjchem-20 122 46     SPACE eurjchem-20 122 47 compound compound NOUN eurjchem-20 122 48     SPACE eurjchem-20 122 49 4j 4j NOUN eurjchem-20 122 50     SPACE eurjchem-20 122 51 showed show VERB eurjchem-20 122 52     SPACE eurjchem-20 122 53 high high ADJ eurjchem-20 122 54     SPACE eurjchem-20 122 55 activity activity NOUN eurjchem-20 122 56     SPACE eurjchem-20 122 57 against against ADP eurjchem-20 122 58     SPACE eurjchem-20 122 59 gram gram NOUN eurjchem-20 122 60     SPACE eurjchem-20 122 61 negative negative ADJ eurjchem-20 122 62     SPACE eurjchem-20 122 63 bacteria bacteria NOUN eurjchem-20 122 64     SPACE eurjchem-20 122 65 ( ( PUNCT eurjchem-20 122 66 k. k. NOUN eurjchem-20 122 67     SPACE eurjchem-20 122 68 pneumoniae pneumoniae NOUN eurjchem-20 122 69 ) ) PUNCT eurjchem-20 122 70 . . PUNCT eurjchem-20 122 71     SPACE eurjchem-20 123 1 the the DET eurjchem-20 123 2     SPACE eurjchem-20 123 3 compounds compound NOUN eurjchem-20 123 4     SPACE eurjchem-20 123 5 4f 4f NOUN eurjchem-20 123 6     SPACE eurjchem-20 123 7 and and CCONJ eurjchem-20 123 8     SPACE eurjchem-20 123 9 4l 4l NOUN eurjchem-20 123 10     SPACE eurjchem-20 123 11 exhibited exhibit VERB eurjchem-20 123 12     SPACE eurjchem-20 123 13 higher high ADJ eurjchem-20 123 14     SPACE eurjchem-20 123 15 activity activity NOUN eurjchem-20 123 16     SPACE eurjchem-20 123 17 against against ADP eurjchem-20 123 18     SPACE eurjchem-20 123 19 escherichia escherichia NOUN eurjchem-20 123 20     SPACE eurjchem-20 123 21 coli coli NOUN eurjchem-20 123 22     SPACE eurjchem-20 123 23 when when SCONJ eurjchem-20 123 24     SPACE eurjchem-20 123 25 compared compare VERB eurjchem-20 123 26     SPACE eurjchem-20 123 27 to to ADP eurjchem-20 123 28     SPACE eurjchem-20 123 29 that that PRON eurjchem-20 123 30     SPACE eurjchem-20 123 31 of of ADP eurjchem-20 123 32     SPACE eurjchem-20 123 33 the the DET eurjchem-20 123 34     SPACE eurjchem-20 123 35 standard standard NOUN eurjchem-20 123 36 . . PUNCT eurjchem-20 123 37     SPACE eurjchem-20 124 1 the the DET eurjchem-20 124 2     SPACE eurjchem-20 124 3 compound compound NOUN eurjchem-20 124 4     SPACE eurjchem-20 124 5 4k 4k NOUN eurjchem-20 124 6     SPACE eurjchem-20 124 7 exhibited exhibit VERB eurjchem-20 124 8     SPACE eurjchem-20 124 9 high high ADJ eurjchem-20 124 10     SPACE eurjchem-20 124 11 activity activity NOUN eurjchem-20 124 12 , , PUNCT eurjchem-20 124 13     SPACE eurjchem-20 124 14 against against ADP eurjchem-20 124 15     SPACE eurjchem-20 124 16 gram gram NOUN eurjchem-20 124 17     SPACE eurjchem-20 124 18 positive positive ADJ eurjchem-20 124 19     SPACE eurjchem-20 124 20 bacterium bacterium NOUN eurjchem-20 124 21     SPACE eurjchem-20 124 22 staphylococcus staphylococcus NOUN eurjchem-20 124 23     SPACE eurjchem-20 124 24 aureus aureus NOUN eurjchem-20 124 25     SPACE eurjchem-20 124 26 when when SCONJ eurjchem-20 124 27     SPACE eurjchem-20 124 28 compared compare VERB eurjchem-20 124 29     SPACE eurjchem-20 124 30 to to ADP eurjchem-20 124 31     SPACE eurjchem-20 124 32 that that PRON eurjchem-20 124 33     SPACE eurjchem-20 124 34 of of ADP eurjchem-20 124 35     SPACE eurjchem-20 124 36 the the DET eurjchem-20 124 37     SPACE eurjchem-20 124 38 ampicillin ampicillin NOUN eurjchem-20 124 39 . . PUNCT eurjchem-20 124 40     SPACE eurjchem-20 124 41 majority majority NOUN eurjchem-20 124 42     SPACE eurjchem-20 124 43 of of ADP eurjchem-20 124 44     SPACE eurjchem-20 124 45 the the DET eurjchem-20 124 46     SPACE eurjchem-20 124 47 compounds compound NOUN eurjchem-20 124 48     SPACE eurjchem-20 124 49 exhibited exhibit VERB eurjchem-20 124 50     SPACE eurjchem-20 124 51 significant significant ADJ eurjchem-20 124 52     SPACE eurjchem-20 124 53 antibacterial antibacterial ADJ eurjchem-20 124 54     SPACE eurjchem-20 124 55 activity activity NOUN eurjchem-20 124 56     SPACE eurjchem-20 124 57 ( ( PUNCT eurjchem-20 124 58 table table NOUN eurjchem-20 124 59     SPACE eurjchem-20 124 60 1 1 NUM eurjchem-20 124 61 ) ) PUNCT eurjchem-20 124 62 . . PUNCT eurjchem-20 124 63     SPACE eurjchem-20 125 1 majority majority NOUN eurjchem-20 125 2     SPACE eurjchem-20 125 3 of of ADP eurjchem-20 125 4     SPACE eurjchem-20 125 5 the the DET eurjchem-20 125 6     SPACE eurjchem-20 125 7 compounds compound NOUN eurjchem-20 125 8     SPACE eurjchem-20 125 9 showed show VERB eurjchem-20 125 10     SPACE eurjchem-20 125 11 significant significant ADJ eurjchem-20 125 12     SPACE eurjchem-20 125 13 activities activity NOUN eurjchem-20 125 14     SPACE eurjchem-20 125 15 for for ADP eurjchem-20 125 16     SPACE eurjchem-20 125 17 dpph dpph PROPN eurjchem-20 125 18     SPACE eurjchem-20 125 19 radical radical ADJ eurjchem-20 125 20     SPACE eurjchem-20 125 21 scavenging scavenging NOUN eurjchem-20 125 22     SPACE eurjchem-20 125 23 when when SCONJ eurjchem-20 125 24     SPACE eurjchem-20 125 25 compared compare VERB eurjchem-20 125 26     SPACE eurjchem-20 125 27 to to PART eurjchem-20 125 28     SPACE eurjchem-20 125 29 stavudine stavudine VERB eurjchem-20 125 30     SPACE eurjchem-20 125 31 and and CCONJ eurjchem-20 125 32     SPACE eurjchem-20 125 33 vitamin vitamin NOUN eurjchem-20 125 34     SPACE eurjchem-20 125 35 c c NOUN eurjchem-20 125 36     SPACE eurjchem-20 125 37 ( ( PUNCT eurjchem-20 125 38 table table NOUN eurjchem-20 125 39     SPACE eurjchem-20 125 40 2 2 NUM eurjchem-20 125 41 ) ) PUNCT eurjchem-20 125 42 . . PUNCT eurjchem-20 125 43     SPACE eurjchem-20 126 1 the the DET eurjchem-20 126 2     SPACE eurjchem-20 126 3 potency potency NOUN eurjchem-20 126 4     SPACE eurjchem-20 126 5 of of ADP eurjchem-20 126 6     SPACE eurjchem-20 126 7 these these DET eurjchem-20 126 8     SPACE eurjchem-20 126 9 radical radical ADJ eurjchem-20 126 10     SPACE eurjchem-20 126 11 scavenging scavenge VERB eurjchem-20 126 12     SPACE eurjchem-20 126 13 activities activity NOUN eurjchem-20 126 14     SPACE eurjchem-20 126 15 was be AUX eurjchem-20 126 16     SPACE eurjchem-20 126 17 mainly mainly ADV eurjchem-20 126 18     SPACE eurjchem-20 126 19 influenced influence VERB eurjchem-20 126 20     SPACE eurjchem-20 126 21 by by ADP eurjchem-20 126 22     SPACE eurjchem-20 126 23 the the DET eurjchem-20 126 24     SPACE eurjchem-20 126 25 fragments fragment NOUN eurjchem-20 126 26     SPACE eurjchem-20 126 27 attached attach VERB eurjchem-20 126 28     SPACE eurjchem-20 126 29 to to ADP eurjchem-20 126 30     SPACE eurjchem-20 126 31 the the DET eurjchem-20 126 32     SPACE eurjchem-20 126 33 phosphorylated phosphorylate VERB eurjchem-20 126 34     SPACE eurjchem-20 126 35 stavudine stavudine NOUN eurjchem-20 126 36 . . PUNCT eurjchem-20 126 37     SPACE eurjchem-20 127 1 the the DET eurjchem-20 127 2     SPACE eurjchem-20 127 3 fragments fragment NOUN eurjchem-20 127 4     SPACE eurjchem-20 127 5 4‐nitrophenyl 4‐nitrophenyl NUM eurjchem-20 127 6     SPACE eurjchem-20 127 7 phosphoryl phosphoryl NOUN eurjchem-20 127 8     SPACE eurjchem-20 127 9 moiety moiety NOUN eurjchem-20 127 10     SPACE eurjchem-20 127 11 and and CCONJ eurjchem-20 127 12     SPACE eurjchem-20 127 13 various various ADJ eurjchem-20 127 14     SPACE eurjchem-20 127 15 cyclic cyclic ADJ eurjchem-20 127 16     SPACE eurjchem-20 127 17 amines amine NOUN eurjchem-20 127 18     SPACE eurjchem-20 127 19 and and CCONJ eurjchem-20 127 20     SPACE eurjchem-20 127 21 amino amino NOUN eurjchem-20 127 22     SPACE eurjchem-20 127 23 acid acid NOUN eurjchem-20 127 24     SPACE eurjchem-20 127 25 esters ester NOUN eurjchem-20 127 26     SPACE eurjchem-20 127 27 linked link VERB eurjchem-20 127 28     SPACE eurjchem-20 127 29 to to AUX eurjchem-20 127 30     SPACE eurjchem-20 127 31 phosphorus phosphorus NOUN eurjchem-20 127 32     SPACE eurjchem-20 127 33 led lead VERB eurjchem-20 127 34     SPACE eurjchem-20 127 35 to to PART eurjchem-20 127 36     SPACE eurjchem-20 127 37 increase increase VERB eurjchem-20 127 38     SPACE eurjchem-20 127 39 in in ADP eurjchem-20 127 40     SPACE eurjchem-20 127 41 dpph dpph NOUN eurjchem-20 127 42     SPACE eurjchem-20 127 43 radical radical ADJ eurjchem-20 127 44     SPACE eurjchem-20 127 45 scavenging scavenge VERB eurjchem-20 127 46     SPACE eurjchem-20 127 47 activity activity NOUN eurjchem-20 127 48     SPACE eurjchem-20 127 49 ( ( PUNCT eurjchem-20 127 50 i.e. i.e. X eurjchem-20 127 51     SPACE eurjchem-20 127 52 4e 4e NOUN eurjchem-20 127 53     SPACE eurjchem-20 127 54 and and CCONJ eurjchem-20 127 55     SPACE eurjchem-20 127 56 4i 4i NOUN eurjchem-20 127 57 ) ) PUNCT eurjchem-20 127 58 . . PUNCT eurjchem-20 127 59     SPACE eurjchem-20 128 1 4‐nitrophenyl 4‐nitrophenyl NUM eurjchem-20 128 2     SPACE eurjchem-20 128 3 phosphoryl phosphoryl NOUN eurjchem-20 128 4     SPACE eurjchem-20 128 5 and and CCONJ eurjchem-20 128 6     SPACE eurjchem-20 128 7 phenyl phenyl NOUN eurjchem-20 128 8     SPACE eurjchem-20 128 9 glycine glycine NOUN eurjchem-20 128 10     SPACE eurjchem-20 128 11 ethyl ethyl PROPN eurjchem-20 128 12     SPACE eurjchem-20 128 13 ester ester NOUN eurjchem-20 128 14     SPACE eurjchem-20 128 15 moieties moiety NOUN eurjchem-20 128 16     SPACE eurjchem-20 128 17 were be AUX eurjchem-20 128 18     SPACE eurjchem-20 128 19 found find VERB eurjchem-20 128 20     SPACE eurjchem-20 128 21 to to PART eurjchem-20 128 22     SPACE eurjchem-20 128 23 be be AUX eurjchem-20 128 24     SPACE eurjchem-20 128 25 the the DET eurjchem-20 128 26     SPACE eurjchem-20 128 27 most most ADJ eurjchem-20 128 28     SPACE eurjchem-20 128 29 potent potent NOUN eurjchem-20 128 30     SPACE eurjchem-20 128 31 fragments fragment NOUN eurjchem-20 128 32     SPACE eurjchem-20 128 33 for for ADP eurjchem-20 128 34     SPACE eurjchem-20 128 35 increasing increase VERB eurjchem-20 128 36     SPACE eurjchem-20 128 37 radical radical ADJ eurjchem-20 128 38     SPACE eurjchem-20 128 39 scavenging scavenging ADJ eurjchem-20 128 40     SPACE eurjchem-20 128 41 activity activity NOUN eurjchem-20 128 42 . . PUNCT eurjchem-20 128 43         SPACE eurjchem-20 129 1 4 4 NUM eurjchem-20 129 2 . . PUNCT eurjchem-20 129 3     SPACE eurjchem-20 129 4 conclusion conclusion NOUN eurjchem-20 129 5         SPACE eurjchem-20 129 6 in in ADP eurjchem-20 129 7     SPACE eurjchem-20 129 8 conclusion conclusion NOUN eurjchem-20 129 9 , , PUNCT eurjchem-20 129 10     SPACE eurjchem-20 129 11 a a DET eurjchem-20 129 12     SPACE eurjchem-20 129 13 series series NOUN eurjchem-20 129 14     SPACE eurjchem-20 129 15 of of ADP eurjchem-20 129 16     SPACE eurjchem-20 129 17 novel novel NOUN eurjchem-20 129 18     SPACE eurjchem-20 129 19 phosphorylated phosphorylate VERB eurjchem-20 129 20     SPACE eurjchem-20 129 21 derivatives derivative NOUN eurjchem-20 129 22     SPACE eurjchem-20 129 23 of of ADP eurjchem-20 129 24     SPACE eurjchem-20 129 25 stavudine stavudine NOUN eurjchem-20 129 26     SPACE eurjchem-20 129 27 were be AUX eurjchem-20 129 28     SPACE eurjchem-20 129 29 synthesized synthesize VERB eurjchem-20 129 30     SPACE eurjchem-20 129 31 and and CCONJ eurjchem-20 129 32     SPACE eurjchem-20 129 33 evaluated evaluate VERB eurjchem-20 129 34     SPACE eurjchem-20 129 35 for for ADP eurjchem-20 129 36     SPACE eurjchem-20 129 37 their their PRON eurjchem-20 129 38     SPACE eurjchem-20 129 39 antimicrobial antimicrobial ADJ eurjchem-20 129 40     SPACE eurjchem-20 129 41 and and CCONJ eurjchem-20 129 42     SPACE eurjchem-20 129 43 antioxidant antioxidant ADJ eurjchem-20 129 44     SPACE eurjchem-20 129 45 properties property NOUN eurjchem-20 129 46 . . PUNCT eurjchem-20 129 47     SPACE eurjchem-20 129 48 structure structure NOUN eurjchem-20 129 49     SPACE eurjchem-20 129 50 activity activity NOUN eurjchem-20 129 51     SPACE eurjchem-20 129 52 studies study NOUN eurjchem-20 129 53     SPACE eurjchem-20 129 54 showed show VERB eurjchem-20 129 55     SPACE eurjchem-20 129 56 that that SCONJ eurjchem-20 129 57     SPACE eurjchem-20 129 58 the the DET eurjchem-20 129 59     SPACE eurjchem-20 129 60 antioxidant antioxidant NOUN eurjchem-20 129 61     SPACE eurjchem-20 129 62 and and CCONJ eurjchem-20 129 63     SPACE eurjchem-20 129 64 antimicrobial antimicrobial ADJ eurjchem-20 129 65     SPACE eurjchem-20 129 66 potency potency NOUN eurjchem-20 129 67     SPACE eurjchem-20 129 68 was be AUX eurjchem-20 129 69     SPACE eurjchem-20 129 70 mainly mainly ADV eurjchem-20 129 71     SPACE eurjchem-20 129 72 influenced influence VERB eurjchem-20 129 73     SPACE eurjchem-20 129 74 by by ADP eurjchem-20 129 75     SPACE eurjchem-20 129 76 the the DET eurjchem-20 129 77     SPACE eurjchem-20 129 78 functional functional ADJ eurjchem-20 129 79     SPACE eurjchem-20 129 80 groups group NOUN eurjchem-20 129 81     SPACE eurjchem-20 129 82 at at ADP eurjchem-20 129 83     SPACE eurjchem-20 129 84 the the DET eurjchem-20 129 85     SPACE eurjchem-20 129 86 end end NOUN eurjchem-20 129 87     SPACE eurjchem-20 129 88 of of ADP eurjchem-20 129 89     SPACE eurjchem-20 129 90 the the DET eurjchem-20 129 91     SPACE eurjchem-20 129 92 aliphatic aliphatic ADJ eurjchem-20 129 93     SPACE eurjchem-20 129 94 chain chain NOUN eurjchem-20 129 95 , , PUNCT eurjchem-20 129 96     SPACE eurjchem-20 129 97 as as ADV eurjchem-20 129 98     SPACE eurjchem-20 129 99 well well ADV eurjchem-20 129 100     SPACE eurjchem-20 129 101 as as ADP eurjchem-20 129 102     SPACE eurjchem-20 129 103 the the DET eurjchem-20 129 104     SPACE eurjchem-20 129 105 nature nature NOUN eurjchem-20 129 106     SPACE eurjchem-20 129 107 of of ADP eurjchem-20 129 108     SPACE eurjchem-20 129 109 atom atom NOUN eurjchem-20 129 110     SPACE eurjchem-20 129 111 attached attach VERB eurjchem-20 129 112     SPACE eurjchem-20 129 113 directly directly ADV eurjchem-20 129 114     SPACE eurjchem-20 129 115 to to PART eurjchem-20 129 116     SPACE eurjchem-20 129 117 phosphorus phosphorus NOUN eurjchem-20 129 118     SPACE eurjchem-20 129 119 atom atom NOUN eurjchem-20 129 120     SPACE eurjchem-20 129 121 and and CCONJ eurjchem-20 129 122     SPACE eurjchem-20 129 123 the the DET eurjchem-20 129 124     SPACE eurjchem-20 129 125 two two NUM eurjchem-20 129 126     SPACE eurjchem-20 129 127 different different ADJ eurjchem-20 129 128     SPACE eurjchem-20 129 129 types type NOUN eurjchem-20 129 130     SPACE eurjchem-20 129 131 of of ADP eurjchem-20 129 132     SPACE eurjchem-20 129 133 r r NOUN eurjchem-20 129 134     SPACE eurjchem-20 129 135 fragments fragment NOUN eurjchem-20 129 136     SPACE eurjchem-20 129 137 attached attach VERB eurjchem-20 129 138     SPACE eurjchem-20 129 139 to to ADP eurjchem-20 129 140     SPACE eurjchem-20 129 141 phosphorus phosphorus NOUN eurjchem-20 129 142     SPACE eurjchem-20 129 143 atom atom NOUN eurjchem-20 129 144 , , PUNCT eurjchem-20 129 145     SPACE eurjchem-20 129 146 which which PRON eurjchem-20 129 147     SPACE eurjchem-20 129 148 provided provide VERB eurjchem-20 129 149     SPACE eurjchem-20 129 150 additional additional ADJ eurjchem-20 129 151     SPACE eurjchem-20 129 152 sites site NOUN eurjchem-20 129 153     SPACE eurjchem-20 129 154 of of ADP eurjchem-20 129 155     SPACE eurjchem-20 129 156 interactions interaction NOUN eurjchem-20 129 157     SPACE eurjchem-20 129 158 between between ADP eurjchem-20 129 159     SPACE eurjchem-20 129 160 the the DET eurjchem-20 129 161     SPACE eurjchem-20 129 162 inhibitor inhibitor NOUN eurjchem-20 129 163     SPACE eurjchem-20 129 164 and and CCONJ eurjchem-20 129 165     SPACE eurjchem-20 129 166 the the DET eurjchem-20 129 167     SPACE eurjchem-20 129 168 enzyme enzyme NOUN eurjchem-20 129 169 , , PUNCT eurjchem-20 129 170     SPACE eurjchem-20 129 171 which which PRON eurjchem-20 129 172     SPACE eurjchem-20 129 173 constitutes constitute VERB eurjchem-20 129 174     SPACE eurjchem-20 129 175 a a DET eurjchem-20 129 176     SPACE eurjchem-20 129 177 key key ADJ eurjchem-20 129 178     SPACE eurjchem-20 129 179 element element NOUN eurjchem-20 129 180     SPACE eurjchem-20 129 181 for for ADP eurjchem-20 129 182     SPACE eurjchem-20 129 183 enhanced enhance VERB eurjchem-20 129 184     SPACE eurjchem-20 129 185 affinity affinity NOUN eurjchem-20 129 186 . . PUNCT eurjchem-20 129 187     SPACE eurjchem-20 130 1 the the DET eurjchem-20 130 2     SPACE eurjchem-20 130 3 results result NOUN eurjchem-20 130 4     SPACE eurjchem-20 130 5 suggest suggest VERB eurjchem-20 130 6     SPACE eurjchem-20 130 7 that that SCONJ eurjchem-20 130 8     SPACE eurjchem-20 130 9 the the DET eurjchem-20 130 10     SPACE eurjchem-20 130 11 compounds compound NOUN eurjchem-20 130 12     SPACE eurjchem-20 130 13 4e 4e NOUN eurjchem-20 130 14 , , PUNCT eurjchem-20 130 15     SPACE eurjchem-20 130 16 4f 4f NUM eurjchem-20 130 17     SPACE eurjchem-20 130 18 and and CCONJ eurjchem-20 130 19     SPACE eurjchem-20 130 20 4i 4i NOUN eurjchem-20 130 21     SPACE eurjchem-20 130 22 showed show VERB eurjchem-20 130 23     SPACE eurjchem-20 130 24 promising promising ADJ eurjchem-20 130 25     SPACE eurjchem-20 130 26 antioxidant antioxidant ADJ eurjchem-20 130 27     SPACE eurjchem-20 130 28 activities activity NOUN eurjchem-20 130 29 . . PUNCT eurjchem-20 130 30           SPACE eurjchem-20 131 1 acknowledgement acknowledgement NOUN eurjchem-20 131 2         SPACE eurjchem-20 131 3 we we PRON eurjchem-20 131 4     SPACE eurjchem-20 131 5 thank thank VERB eurjchem-20 131 6     SPACE eurjchem-20 131 7 brns brn NOUN eurjchem-20 131 8     SPACE eurjchem-20 131 9 ( ( PUNCT eurjchem-20 131 10 dae dae NOUN eurjchem-20 131 11 ) ) PUNCT eurjchem-20 131 12 , , PUNCT eurjchem-20 131 13     SPACE eurjchem-20 131 14 barc barc PROPN eurjchem-20 131 15 , , PUNCT eurjchem-20 131 16     SPACE eurjchem-20 131 17 mumbai mumbai NOUN eurjchem-20 131 18     SPACE eurjchem-20 131 19 for for ADP eurjchem-20 131 20     SPACE eurjchem-20 131 21 the the DET eurjchem-20 131 22     SPACE eurjchem-20 131 23 financial financial ADJ eurjchem-20 131 24     SPACE eurjchem-20 131 25 support support NOUN eurjchem-20 131 26     SPACE eurjchem-20 131 27 ( ( PUNCT eurjchem-20 131 28 project project NOUN eurjchem-20 131 29     SPACE eurjchem-20 131 30 no no NOUN eurjchem-20 131 31 . . PUNCT eurjchem-20 131 32 : : PUNCT eurjchem-20 131 33     SPACE eurjchem-20 131 34 ( ( PUNCT eurjchem-20 131 35 2007/37/46 2007/37/46 NUM eurjchem-20 131 36 / / SYM eurjchem-20 131 37 brns/2916 brns/2916 PROPN eurjchem-20 131 38 ) ) PUNCT eurjchem-20 131 39 , , PUNCT eurjchem-20 131 40     SPACE eurjchem-20 131 41 dated date VERB eurjchem-20 131 42     SPACE eurjchem-20 131 43 31‐03‐ 31‐03‐ NUM eurjchem-20 131 44 2008 2008 NUM eurjchem-20 131 45 . . PUNCT eurjchem-20 131 46         SPACE eurjchem-20 132 1 references reference NOUN eurjchem-20 132 2         SPACE eurjchem-20 132 3 [ [ X eurjchem-20 132 4 1 1 NUM eurjchem-20 132 5 ] ] PUNCT eurjchem-20 132 6 . . PUNCT eurjchem-20 133 1 browne browne PROPN eurjchem-20 133 2 , , PUNCT eurjchem-20 133 3     SPACE eurjchem-20 133 4 m. m. NOUN eurjchem-20 133 5     SPACE eurjchem-20 133 6 j. j. PROPN eurjchem-20 133 7 ; ; PUNCT eurjchem-20 133 8     SPACE eurjchem-20 133 9 mayer mayer PROPN eurjchem-20 133 10 , , PUNCT eurjchem-20 133 11     SPACE eurjchem-20 133 12 k. k. PROPN eurjchem-20 133 13     SPACE eurjchem-20 133 14 h. h. PROPN eurjchem-20 133 15 ; ; PUNCT eurjchem-20 133 16     SPACE eurjchem-20 133 17 chafee chafee NOUN eurjchem-20 133 18 , , PUNCT eurjchem-20 133 19     SPACE eurjchem-20 133 20 s. s. PROPN eurjchem-20 133 21     SPACE eurjchem-20 133 22 b. b. PROPN eurjchem-20 133 23     SPACE eurjchem-20 133 24 d. d. PROPN eurjchem-20 133 25 ; ; PUNCT eurjchem-20 133 26     SPACE eurjchem-20 133 27 dudley dudley ADJ eurjchem-20 133 28 , , PUNCT eurjchem-20 133 29     SPACE eurjchem-20 133 30 m. m. NOUN eurjchem-20 133 31     SPACE eurjchem-20 133 32 n. n. NOUN eurjchem-20 133 33 ; ; PUNCT eurjchem-20 133 34     SPACE eurjchem-20 133 35 posner posner NOUN eurjchem-20 133 36 , , PUNCT eurjchem-20 133 37     SPACE eurjchem-20 133 38 m. m. NOUN eurjchem-20 133 39     SPACE eurjchem-20 133 40 r. r. PROPN eurjchem-20 133 41 ; ; PUNCT eurjchem-20 133 42     SPACE eurjchem-20 133 43 steinberg steinberg PROPN eurjchem-20 133 44 , , PUNCT eurjchem-20 133 45     SPACE eurjchem-20 133 46 s. s. PROPN eurjchem-20 133 47     SPACE eurjchem-20 133 48 m. m. NOUN eurjchem-20 133 49 ; ; PUNCT eurjchem-20 133 50     SPACE eurjchem-20 133 51 graham graham PROPN eurjchem-20 133 52 , , PUNCT eurjchem-20 133 53     SPACE eurjchem-20 133 54 k. k. PROPN eurjchem-20 133 55     SPACE eurjchem-20 133 56 k. k. PROPN eurjchem-20 133 57 ; ; PUNCT eurjchem-20 133 58     SPACE eurjchem-20 133 59 geletko geletko PROPN eurjchem-20 133 60 , , PUNCT eurjchem-20 133 61     SPACE eurjchem-20 133 62 s. s. PROPN eurjchem-20 133 63     SPACE eurjchem-20 133 64 m. m. NOUN eurjchem-20 133 65 ; ; PUNCT eurjchem-20 133 66     SPACE eurjchem-20 133 67 zinner zinner NOUN eurjchem-20 133 68 , , PUNCT eurjchem-20 133 69     SPACE eurjchem-20 133 70 s. s. PROPN eurjchem-20 133 71     SPACE eurjchem-20 133 72 h. h. PROPN eurjchem-20 133 73 ; ; PUNCT eurjchem-20 133 74     SPACE eurjchem-20 133 75 denamn denamn ADJ eurjchem-20 133 76 , , PUNCT eurjchem-20 133 77     SPACE eurjchem-20 133 78 s. s. PROPN eurjchem-20 133 79     SPACE eurjchem-20 133 80 l. l. PROPN eurjchem-20 133 81 ; ; PUNCT eurjchem-20 133 82     SPACE eurjchem-20 133 83 dunkle dunkle PROPN eurjchem-20 133 84 , , PUNCT eurjchem-20 133 85     SPACE eurjchem-20 133 86 l. l. PROPN eurjchem-20 133 87     SPACE eurjchem-20 133 88 m. m. NOUN eurjchem-20 133 89 ; ; PUNCT eurjchem-20 133 90     SPACE eurjchem-20 133 91 kaul kaul NOUN eurjchem-20 133 92 , , PUNCT eurjchem-20 133 93     SPACE eurjchem-20 133 94 s. s. PROPN eurjchem-20 133 95 ; ; PUNCT eurjchem-20 133 96       SPACE eurjchem-20 133 97 mclaren mclaren PROPN eurjchem-20 133 98 , , PUNCT eurjchem-20 133 99     SPACE eurjchem-20 133 100 c. c. NOUN eurjchem-20 133 101 ; ; PUNCT eurjchem-20 133 102     SPACE eurjchem-20 133 103 skowron skowron NOUN eurjchem-20 133 104 , , PUNCT eurjchem-20 133 105     SPACE eurjchem-20 133 106 g. g. NOUN eurjchem-20 133 107 ; ; PUNCT eurjchem-20 133 108       SPACE eurjchem-20 133 109 kouttab kouttab PROPN eurjchem-20 133 110 , , PUNCT eurjchem-20 133 111     SPACE eurjchem-20 133 112 n. n. NOUN eurjchem-20 133 113     SPACE eurjchem-20 133 114 m. m. NOUN eurjchem-20 133 115 ; ; PUNCT eurjchem-20 133 116     SPACE eurjchem-20 133 117 kennedy kennedy PROPN eurjchem-20 133 118 , , PUNCT eurjchem-20 133 119     SPACE eurjchem-20 133 120 t. t. PROPN eurjchem-20 133 121     SPACE eurjchem-20 133 122 a. a. NOUN eurjchem-20 133 123 ; ; PUNCT eurjchem-20 133 124     SPACE eurjchem-20 133 125 weitberg weitberg PROPN eurjchem-20 133 126 , , PUNCT eurjchem-20 133 127     SPACE eurjchem-20 133 128 a. a. NOUN eurjchem-20 133 129     SPACE eurjchem-20 133 130 b. b. PROPN eurjchem-20 133 131 ; ; PUNCT eurjchem-20 133 132     SPACE eurjchem-20 133 133 curt curt NOUN eurjchem-20 133 134 , , PUNCT eurjchem-20 133 135     SPACE eurjchem-20 133 136 g. g. NOUN eurjchem-20 133 137     SPACE eurjchem-20 133 138 a. a. PROPN eurjchem-20 133 139     SPACE eurjchem-20 133 140 j. j. PROPN eurjchem-20 133 141     SPACE eurjchem-20 133 142 infect infect VERB eurjchem-20 133 143 . . PUNCT eurjchem-20 133 144     SPACE eurjchem-20 134 1 dis dis PROPN eurjchem-20 134 2 . . PUNCT eurjchem-20 134 3     SPACE eurjchem-20 135 1 1993 1993 NUM eurjchem-20 135 2 , , PUNCT eurjchem-20 135 3     SPACE eurjchem-20 135 4 167 167 NUM eurjchem-20 135 5 , , PUNCT eurjchem-20 135 6     SPACE eurjchem-20 135 7 21 21 NUM eurjchem-20 135 8 – – PUNCT eurjchem-20 135 9 29 29 NUM eurjchem-20 135 10 . . PUNCT eurjchem-20 136 1 [ [ X eurjchem-20 136 2 2 2 NUM eurjchem-20 136 3 ] ] PUNCT eurjchem-20 136 4 . . PUNCT eurjchem-20 137 1 murray murray PROPN eurjchem-20 137 2 , , PUNCT eurjchem-20 137 3     SPACE eurjchem-20 137 4 h. h. PROPN eurjchem-20 137 5     SPACE eurjchem-20 137 6 w. w. PROPN eurjchem-20 137 7 ; ; PUNCT eurjchem-20 137 8     SPACE eurjchem-20 137 9 squires squire NOUN eurjchem-20 137 10 , , PUNCT eurjchem-20 137 11     SPACE eurjchem-20 137 12 k. k. PROPN eurjchem-20 137 13     SPACE eurjchem-20 137 14 e. e. PROPN eurjchem-20 137 15 ; ; PUNCT eurjchem-20 137 16     SPACE eurjchem-20 137 17 weiss weiss PROPN eurjchem-20 137 18 , , PUNCT eurjchem-20 137 19     SPACE eurjchem-20 137 20 w. w. NOUN eurjchem-20 137 21 ; ; PUNCT eurjchem-20 137 22     SPACE eurjchem-20 137 23 sledz sledz NOUN eurjchem-20 137 24 , , PUNCT eurjchem-20 137 25     SPACE eurjchem-20 137 26 s. s. PROPN eurjchem-20 137 27 ; ; PUNCT eurjchem-20 137 28     SPACE eurjchem-20 137 29 sacks sack NOUN eurjchem-20 137 30 , , PUNCT eurjchem-20 137 31     SPACE eurjchem-20 137 32 h. h. PROPN eurjchem-20 137 33     SPACE eurjchem-20 137 34 s. s. PROPN eurjchem-20 137 35 ; ; PUNCT eurjchem-20 137 36       SPACE eurjchem-20 137 37 hassett hassett NOUN eurjchem-20 137 38 , , PUNCT eurjchem-20 137 39     SPACE eurjchem-20 137 40 j. j. PROPN eurjchem-20 137 41 ; ; PUNCT eurjchem-20 137 42     SPACE eurjchem-20 137 43 cross cross NOUN eurjchem-20 137 44 , , PUNCT eurjchem-20 137 45     SPACE eurjchem-20 137 46 a. a. NOUN eurjchem-20 137 47 ; ; PUNCT eurjchem-20 137 48     SPACE eurjchem-20 137 49 anderson anderson PROPN eurjchem-20 137 50 , , PUNCT eurjchem-20 137 51     SPACE eurjchem-20 137 52 r. r. PROPN eurjchem-20 137 53     SPACE eurjchem-20 137 54 e. e. PROPN eurjchem-20 137 55 ; ; PUNCT eurjchem-20 137 56     SPACE eurjchem-20 137 57 dunkle dunkle PROPN eurjchem-20 137 58 , , PUNCT eurjchem-20 137 59     SPACE eurjchem-20 137 60 l. l. PROPN eurjchem-20 137 61     SPACE eurjchem-20 137 62 m. m. PROPN eurjchem-20 137 63       SPACE eurjchem-20 137 64 j. j. PROPN eurjchem-20 137 65     SPACE eurjchem-20 137 66 infect infect VERB eurjchem-20 137 67 . . PUNCT eurjchem-20 137 68     SPACE eurjchem-20 138 1 dis dis PROPN eurjchem-20 138 2 . . PUNCT eurjchem-20 138 3     SPACE eurjchem-20 139 1 1995 1995 NUM eurjchem-20 139 2 , , PUNCT eurjchem-20 139 3     SPACE eurjchem-20 139 4 171(2 171(2 NUM eurjchem-20 139 5 ) ) PUNCT eurjchem-20 139 6 , , PUNCT eurjchem-20 139 7     SPACE eurjchem-20 139 8 123–130 123–130 NUM eurjchem-20 139 9 . . PUNCT eurjchem-20 140 1 [ [ X eurjchem-20 140 2 3 3 NUM eurjchem-20 140 3 ] ] PUNCT eurjchem-20 140 4 . . PUNCT eurjchem-20 141 1 balzarini balzarini PROPN eurjchem-20 141 2 , , PUNCT eurjchem-20 141 3     SPACE eurjchem-20 141 4 j. j. PROPN eurjchem-20 141 5 ; ; PUNCT eurjchem-20 141 6     SPACE eurjchem-20 141 7 herdewijn herdewijn NOUN eurjchem-20 141 8 , , PUNCT eurjchem-20 141 9     SPACE eurjchem-20 141 10 p. p. NOUN eurjchem-20 141 11 ; ; PUNCT eurjchem-20 141 12     SPACE eurjchem-20 141 13 clercq clercq NOUN eurjchem-20 141 14 , , PUNCT eurjchem-20 141 15     SPACE eurjchem-20 141 16 e. e. PROPN eurjchem-20 141 17     SPACE eurjchem-20 141 18 d. d. PROPN eurjchem-20 141 19     SPACE eurjchem-20 141 20 j. j. PROPN eurjchem-20 141 21     SPACE eurjchem-20 141 22 biol biol PROPN eurjchem-20 141 23 . . PUNCT eurjchem-20 141 24     SPACE eurjchem-20 141 25 chem chem NOUN eurjchem-20 141 26 . . PUNCT eurjchem-20 141 27     SPACE eurjchem-20 141 28 1989 1989 NUM eurjchem-20 141 29 , , PUNCT eurjchem-20 141 30     SPACE eurjchem-20 141 31 264 264 NUM eurjchem-20 141 32 , , PUNCT eurjchem-20 141 33     SPACE eurjchem-20 141 34 6127 6127 NUM eurjchem-20 141 35 – – PUNCT eurjchem-20 141 36 6133 6133 NUM eurjchem-20 141 37 . . PUNCT eurjchem-20 141 38     SPACE eurjchem-20 142 1 [ [ X eurjchem-20 142 2 4 4 NUM eurjchem-20 142 3 ] ] PUNCT eurjchem-20 142 4 . . PUNCT eurjchem-20 143 1 ho ho PROPN eurjchem-20 143 2 , , PUNCT eurjchem-20 143 3     SPACE eurjchem-20 143 4 h.‐t h.‐t PROPN eurjchem-20 143 5 . . PROPN eurjchem-20 143 6 ; ; PUNCT eurjchem-20 143 7     SPACE eurjchem-20 143 8 hitchcock hitchcock NOUN eurjchem-20 143 9 , , PUNCT eurjchem-20 143 10     SPACE eurjchem-20 143 11 m. m. NOUN eurjchem-20 143 12     SPACE eurjchem-20 143 13 j. j. PROPN eurjchem-20 143 14     SPACE eurjchem-20 143 15 m. m. NOUN eurjchem-20 143 16     SPACE eurjchem-20 143 17 antimicrob antimicrob PROPN eurjchem-20 143 18 . . PUNCT eurjchem-20 143 19     SPACE eurjchem-20 144 1 agents agents PROPN eurjchem-20 144 2     SPACE eurjchem-20 144 3 chemother chemother PROPN eurjchem-20 144 4 . . PUNCT eurjchem-20 144 5     SPACE eurjchem-20 145 1 1989 1989 NUM eurjchem-20 145 2 , , PUNCT eurjchem-20 145 3     SPACE eurjchem-20 145 4 33 33 NUM eurjchem-20 145 5 , , PUNCT eurjchem-20 145 6     SPACE eurjchem-20 145 7 844–849 844–849 NUM eurjchem-20 145 8 . . PUNCT eurjchem-20 145 9       SPACE eurjchem-20 146 1 [ [ X eurjchem-20 146 2 5 5 NUM eurjchem-20 146 3 ] ] PUNCT eurjchem-20 146 4 . . PUNCT eurjchem-20 147 1 mansuri mansuri PROPN eurjchem-20 147 2 , , PUNCT eurjchem-20 147 3     SPACE eurjchem-20 147 4 m. m. NOUN eurjchem-20 147 5     SPACE eurjchem-20 147 6 m. m. NOUN eurjchem-20 147 7 ; ; PUNCT eurjchem-20 147 8     SPACE eurjchem-20 147 9 starrett starrett PROPN eurjchem-20 147 10 , , PUNCT eurjchem-20 147 11     SPACE eurjchem-20 147 12 j. j. PROPN eurjchem-20 147 13     SPACE eurjchem-20 147 14 e. e. PROPN eurjchem-20 147 15 ; ; PUNCT eurjchem-20 147 16     SPACE eurjchem-20 147 17 ghazzouli ghazzouli PROPN eurjchem-20 147 18 , , PUNCT eurjchem-20 147 19     SPACE eurjchem-20 147 20 i. i. NOUN eurjchem-20 147 21 ; ; PUNCT eurjchem-20 147 22     SPACE eurjchem-20 147 23 hitchcock hitchcock NOUN eurjchem-20 147 24 , , PUNCT eurjchem-20 147 25     SPACE eurjchem-20 147 26 m. m. NOUN eurjchem-20 147 27     SPACE eurjchem-20 147 28 j. j. PROPN eurjchem-20 147 29     SPACE eurjchem-20 147 30 m. m. NOUN eurjchem-20 147 31 ; ; PUNCT eurjchem-20 147 32     SPACE eurjchem-20 147 33 sterzycki sterzycki PROPN eurjchem-20 147 34 , , PUNCT eurjchem-20 147 35     SPACE eurjchem-20 147 36 r. r. PROPN eurjchem-20 147 37     SPACE eurjchem-20 147 38 z. z. PROPN eurjchem-20 147 39 ; ; PUNCT eurjchem-20 147 40     SPACE eurjchem-20 147 41 brankovan brankovan NOUN eurjchem-20 147 42 , , PUNCT eurjchem-20 147 43     SPACE eurjchem-20 147 44 v. v. PROPN eurjchem-20 147 45 ; ; PUNCT eurjchem-20 147 46     SPACE eurjchem-20 147 47 lin lin PROPN eurjchem-20 147 48 , , PUNCT eurjchem-20 147 49     SPACE eurjchem-20 147 50 t.‐s t.‐s PROPN eurjchem-20 147 51 . . PUNCT eurjchem-20 147 52 ; ; PUNCT eurjchem-20 147 53     SPACE eurjchem-20 147 54 august august PROPN eurjchem-20 147 55 , , PUNCT eurjchem-20 147 56     SPACE eurjchem-20 147 57 e. e. PROPN eurjchem-20 147 58     SPACE eurjchem-20 147 59 m. m. NOUN eurjchem-20 147 60 ; ; PUNCT eurjchem-20 147 61     SPACE eurjchem-20 147 62 prussoff prussoff NOUN eurjchem-20 147 63 , , PUNCT eurjchem-20 147 64     SPACE eurjchem-20 147 65 w. w. PROPN eurjchem-20 147 66     SPACE eurjchem-20 147 67 h. h. PROPN eurjchem-20 147 68 ; ; PUNCT eurjchem-20 147 69     SPACE eurjchem-20 147 70 sommadossi sommadossi ADJ eurjchem-20 147 71 , , PUNCT eurjchem-20 147 72     SPACE eurjchem-20 147 73 j.‐p j.‐p PROPN eurjchem-20 147 74 . . PROPN eurjchem-20 147 75 ; ; PUNCT eurjchem-20 147 76     SPACE eurjchem-20 147 77 martin martin PROPN eurjchem-20 147 78 , , PUNCT eurjchem-20 147 79     SPACE eurjchem-20 147 80 j. j. PROPN eurjchem-20 147 81     SPACE eurjchem-20 147 82 c. c. PROPN eurjchem-20 147 83     SPACE eurjchem-20 147 84 j. j. PROPN eurjchem-20 147 85     SPACE eurjchem-20 147 86 med med PROPN eurjchem-20 147 87 . . PUNCT eurjchem-20 147 88     SPACE eurjchem-20 147 89 chem chem NOUN eurjchem-20 147 90 . . PUNCT eurjchem-20 147 91     SPACE eurjchem-20 147 92 1989 1989 NUM eurjchem-20 147 93 , , PUNCT eurjchem-20 147 94     SPACE eurjchem-20 147 95 32 32 NUM eurjchem-20 147 96 , , PUNCT eurjchem-20 147 97     SPACE eurjchem-20 147 98 461–466 461–466 NUM eurjchem-20 147 99 . . PUNCT eurjchem-20 147 100     SPACE eurjchem-20 148 1 [ [ X eurjchem-20 148 2 6 6 NUM eurjchem-20 148 3 ] ] PUNCT eurjchem-20 148 4 . . PUNCT eurjchem-20 149 1 siddiqui siddiqui NOUN eurjchem-20 149 2 , , PUNCT eurjchem-20 149 3     SPACE eurjchem-20 149 4 a. a. NOUN eurjchem-20 149 5     SPACE eurjchem-20 149 6 q. q. PROPN eurjchem-20 149 7 ; ; PUNCT eurjchem-20 149 8     SPACE eurjchem-20 149 9 mcguigan mcguigan PROPN eurjchem-20 149 10 , , PUNCT eurjchem-20 149 11     SPACE eurjchem-20 149 12 c. c. NOUN eurjchem-20 149 13 ; ; PUNCT eurjchem-20 149 14     SPACE eurjchem-20 149 15 ballatore ballatore NOUN eurjchem-20 149 16 , , PUNCT eurjchem-20 149 17     SPACE eurjchem-20 149 18 c. c. NOUN eurjchem-20 149 19 ; ; PUNCT eurjchem-20 149 20     SPACE eurjchem-20 149 21 zuccotto zuccotto NOUN eurjchem-20 149 22 , , PUNCT eurjchem-20 149 23     SPACE eurjchem-20 149 24 f. f. PROPN eurjchem-20 149 25 ; ; PUNCT eurjchem-20 149 26     SPACE eurjchem-20 149 27 gilbert gilbert PROPN eurjchem-20 149 28 , , PUNCT eurjchem-20 149 29     SPACE eurjchem-20 149 30 i. i. PROPN eurjchem-20 149 31     SPACE eurjchem-20 149 32 h. h. PROPN eurjchem-20 149 33 ; ; PUNCT eurjchem-20 149 34     SPACE eurjchem-20 149 35 de de PROPN eurjchem-20 149 36     SPACE eurjchem-20 149 37 clercq clercq NOUN eurjchem-20 149 38 , , PUNCT eurjchem-20 149 39     SPACE eurjchem-20 149 40 e. e. PROPN eurjchem-20 149 41 ; ; PUNCT eurjchem-20 149 42     SPACE eurjchem-20 149 43 balzarini balzarini NOUN eurjchem-20 149 44 , , PUNCT eurjchem-20 149 45     SPACE eurjchem-20 149 46 j. j. PROPN eurjchem-20 149 47     SPACE eurjchem-20 149 48 j. j. PROPN eurjchem-20 149 49     SPACE eurjchem-20 149 50 med med PROPN eurjchem-20 149 51 . . PUNCT eurjchem-20 149 52     SPACE eurjchem-20 149 53 chem chem NOUN eurjchem-20 149 54 . . PUNCT eurjchem-20 149 55     SPACE eurjchem-20 149 56 1999 1999 NUM eurjchem-20 149 57 , , PUNCT eurjchem-20 149 58     SPACE eurjchem-20 149 59 42 42 NUM eurjchem-20 149 60 , , PUNCT eurjchem-20 149 61     SPACE eurjchem-20 149 62 4122‐4128 4122‐4128 NUM eurjchem-20 149 63 . . PUNCT eurjchem-20 149 64     SPACE eurjchem-20 150 1 [ [ X eurjchem-20 150 2 7 7 NUM eurjchem-20 150 3 ] ] PUNCT eurjchem-20 150 4 . . PUNCT eurjchem-20 151 1 wagner wagner PROPN eurjchem-20 151 2 , , PUNCT eurjchem-20 151 3     SPACE eurjchem-20 151 4 c.r c.r PROPN eurjchem-20 151 5 . . PROPN eurjchem-20 151 6 ; ; PUNCT eurjchem-20 151 7     SPACE eurjchem-20 151 8 iyer iyer NOUN eurjchem-20 151 9 , , PUNCT eurjchem-20 151 10     SPACE eurjchem-20 151 11 v. v. VERB eurjchem-20 151 12     SPACE eurjchem-20 151 13 v. v. NOUN eurjchem-20 151 14 ; ; PUNCT eurjchem-20 151 15     SPACE eurjchem-20 151 16 mcintee mcintee NOUN eurjchem-20 151 17 , , PUNCT eurjchem-20 151 18     SPACE eurjchem-20 151 19 e. e. PROPN eurjchem-20 151 20     SPACE eurjchem-20 151 21 j. j. PROPN eurjchem-20 151 22     SPACE eurjchem-20 151 23 med med PROPN eurjchem-20 151 24 . . PUNCT eurjchem-20 151 25     SPACE eurjchem-20 151 26 res re NOUN eurjchem-20 151 27 . . PUNCT eurjchem-20 151 28     SPACE eurjchem-20 151 29 rev rev VERB eurjchem-20 151 30     SPACE eurjchem-20 151 31 2000 2000 NUM eurjchem-20 151 32 , , PUNCT eurjchem-20 151 33     SPACE eurjchem-20 151 34 20 20 NUM eurjchem-20 151 35 , , PUNCT eurjchem-20 151 36     SPACE eurjchem-20 151 37 417‐451 417‐451 NUM eurjchem-20 151 38 . . PUNCT eurjchem-20 151 39     SPACE eurjchem-20 152 1 [ [ X eurjchem-20 152 2 8 8 NUM eurjchem-20 152 3 ] ] PUNCT eurjchem-20 152 4 . . PUNCT eurjchem-20 153 1 mavromoustakos mavromoustakos PROPN eurjchem-20 153 2 , , PUNCT eurjchem-20 153 3     SPACE eurjchem-20 153 4 t. t. PROPN eurjchem-20 153 5 ; ; PUNCT eurjchem-20 153 6     SPACE eurjchem-20 153 7 calogeropoulou calogeropoulou ADJ eurjchem-20 153 8 , , PUNCT eurjchem-20 153 9     SPACE eurjchem-20 153 10 t. t. NOUN eurjchem-20 153 11 ; ; PUNCT eurjchem-20 153 12     SPACE eurjchem-20 153 13 koufaki koufaki ADJ eurjchem-20 153 14 , , PUNCT eurjchem-20 153 15     SPACE eurjchem-20 153 16 m. m. NOUN eurjchem-20 153 17 ; ; PUNCT eurjchem-20 153 18     SPACE eurjchem-20 153 19 kolocouris kolocouri NOUN eurjchem-20 153 20 , , PUNCT eurjchem-20 153 21     SPACE eurjchem-20 153 22 a. a. NOUN eurjchem-20 153 23 ; ; PUNCT eurjchem-20 153 24     SPACE eurjchem-20 153 25 daliani daliani NOUN eurjchem-20 153 26 , , PUNCT eurjchem-20 153 27     SPACE eurjchem-20 153 28 i. i. NOUN eurjchem-20 153 29 ; ; PUNCT eurjchem-20 153 30     SPACE eurjchem-20 153 31 demetzos demetzos PROPN eurjchem-20 153 32 , , PUNCT eurjchem-20 153 33     SPACE eurjchem-20 153 34 c. c. NOUN eurjchem-20 153 35 ; ; PUNCT eurjchem-20 153 36     SPACE eurjchem-20 153 37 meng meng PROPN eurjchem-20 153 38 , , PUNCT eurjchem-20 153 39     SPACE eurjchem-20 153 40 z. z. PROPN eurjchem-20 153 41 ; ; PUNCT eurjchem-20 153 42     SPACE eurjchem-20 153 43 makriyannis makriyannis NOUN eurjchem-20 153 44 , , PUNCT eurjchem-20 153 45     SPACE eurjchem-20 153 46 a. a. NOUN eurjchem-20 153 47 ; ; PUNCT eurjchem-20 153 48     SPACE eurjchem-20 153 49 balzarini balzarini NOUN eurjchem-20 153 50 , , PUNCT eurjchem-20 153 51     SPACE eurjchem-20 153 52 j. j. PROPN eurjchem-20 153 53 ; ; PUNCT eurjchem-20 153 54     SPACE eurjchem-20 153 55 de de PROPN eurjchem-20 153 56     SPACE eurjchem-20 153 57 clercq clercq NOUN eurjchem-20 153 58 , , PUNCT eurjchem-20 153 59     SPACE eurjchem-20 153 60 e. e. PROPN eurjchem-20 153 61     SPACE eurjchem-20 153 62 j. j. PROPN eurjchem-20 153 63     SPACE eurjchem-20 153 64 med med PROPN eurjchem-20 153 65 . . PUNCT eurjchem-20 153 66     SPACE eurjchem-20 153 67 chem chem NOUN eurjchem-20 153 68 . . PUNCT eurjchem-20 153 69     SPACE eurjchem-20 154 1 2001 2001 NUM eurjchem-20 154 2 , , PUNCT eurjchem-20 154 3     SPACE eurjchem-20 154 4 44 44 NUM eurjchem-20 154 5 , , PUNCT eurjchem-20 154 6     SPACE eurjchem-20 154 7 1702‐1709 1702‐1709 NUM eurjchem-20 154 8 . . PUNCT eurjchem-20 154 9     SPACE eurjchem-20 155 1 [ [ X eurjchem-20 155 2 9 9 NUM eurjchem-20 155 3 ] ] PUNCT eurjchem-20 155 4 . . PUNCT eurjchem-20 155 5 balzarini balzarini PROPN eurjchem-20 155 6 , , PUNCT eurjchem-20 155 7     SPACE eurjchem-20 155 8 j. j. PROPN eurjchem-20 155 9 ; ; PUNCT eurjchem-20 155 10     SPACE eurjchem-20 155 11 aquaro aquaro NOUN eurjchem-20 155 12 , , PUNCT eurjchem-20 155 13     SPACE eurjchem-20 155 14 s. s. PROPN eurjchem-20 155 15 ; ; PUNCT eurjchem-20 155 16     SPACE eurjchem-20 155 17 knispel knispel PROPN eurjchem-20 155 18 , , PUNCT eurjchem-20 155 19     SPACE eurjchem-20 155 20 t. t. PROPN eurjchem-20 155 21 ; ; PUNCT eurjchem-20 155 22     SPACE eurjchem-20 155 23 rampazzo rampazzo NOUN eurjchem-20 155 24 , , PUNCT eurjchem-20 155 25     SPACE eurjchem-20 155 26 c. c. NOUN eurjchem-20 155 27 ; ; PUNCT eurjchem-20 155 28     SPACE eurjchem-20 155 29 bianchi bianchi NOUN eurjchem-20 155 30 , , PUNCT eurjchem-20 155 31     SPACE eurjchem-20 155 32 v. v. PROPN eurjchem-20 155 33 ; ; PUNCT eurjchem-20 155 34     SPACE eurjchem-20 155 35 perno perno NOUN eurjchem-20 155 36 , , PUNCT eurjchem-20 155 37     SPACE eurjchem-20 155 38 c. c. PROPN eurjchem-20 155 39     SPACE eurjchem-20 155 40 f. f. PROPN eurjchem-20 155 41 ; ; PUNCT eurjchem-20 155 42     SPACE eurjchem-20 155 43 de de NOUN eurjchem-20 155 44     SPACE eurjchem-20 155 45 clercq clercq NOUN eurjchem-20 155 46 , , PUNCT eurjchem-20 155 47     SPACE eurjchem-20 155 48 e. e. PROPN eurjchem-20 155 49 ; ; PUNCT eurjchem-20 155 50     SPACE eurjchem-20 155 51 meier meier PROPN eurjchem-20 155 52 , , PUNCT eurjchem-20 155 53     SPACE eurjchem-20 155 54 c. c. PROPN eurjchem-20 155 55     SPACE eurjchem-20 155 56 mol mol PROPN eurjchem-20 155 57 . . PUNCT eurjchem-20 155 58     SPACE eurjchem-20 155 59 pharmacol pharmacol PROPN eurjchem-20 155 60 . . PUNCT eurjchem-20 155 61     SPACE eurjchem-20 155 62 2000 2000 NUM eurjchem-20 155 63 , , PUNCT eurjchem-20 155 64     SPACE eurjchem-20 155 65 58 58 NUM eurjchem-20 155 66 , , PUNCT eurjchem-20 155 67     SPACE eurjchem-20 155 68 928‐35 928‐35 NOUN eurjchem-20 155 69 . . PUNCT eurjchem-20 155 70     SPACE eurjchem-20 156 1 [ [ X eurjchem-20 156 2 10 10 NUM eurjchem-20 156 3 ] ] PUNCT eurjchem-20 156 4 . . PUNCT eurjchem-20 157 1 cardona cardona PROPN eurjchem-20 157 2 , , PUNCT eurjchem-20 157 3     SPACE eurjchem-20 157 4 v. v. NOUN eurjchem-20 157 5     SPACE eurjchem-20 157 6 m. m. NOUN eurjchem-20 157 7 ; ; PUNCT eurjchem-20 157 8     SPACE eurjchem-20 157 9 ayi ayi PROPN eurjchem-20 157 10 , , PUNCT eurjchem-20 157 11     SPACE eurjchem-20 157 12 a. a. NOUN eurjchem-20 157 13     SPACE eurjchem-20 157 14 i. i. PROPN eurjchem-20 157 15 ; ; PUNCT eurjchem-20 157 16     SPACE eurjchem-20 157 17 aubertin aubertin ADJ eurjchem-20 157 18 , , PUNCT eurjchem-20 157 19     SPACE eurjchem-20 157 20 a. a. NOUN eurjchem-20 157 21     SPACE eurjchem-20 157 22 m. m. NOUN eurjchem-20 157 23 ; ; PUNCT eurjchem-20 157 24     SPACE eurjchem-20 157 25 guedj guedj NOUN eurjchem-20 157 26 , , PUNCT eurjchem-20 157 27     SPACE eurjchem-20 157 28 r. r. NOUN eurjchem-20 157 29     SPACE eurjchem-20 157 30 antiviral antiviral NOUN eurjchem-20 157 31     SPACE eurjchem-20 157 32 res re NOUN eurjchem-20 157 33 . . PUNCT eurjchem-20 157 34     SPACE eurjchem-20 157 35 1999 1999 NUM eurjchem-20 157 36 , , PUNCT eurjchem-20 157 37     SPACE eurjchem-20 157 38 42,189‐196 42,189‐196 PROPN eurjchem-20 157 39 . . PUNCT eurjchem-20 157 40     SPACE eurjchem-20 158 1 [ [ X eurjchem-20 158 2 11 11 NUM eurjchem-20 158 3 ] ] PUNCT eurjchem-20 158 4 . . PUNCT eurjchem-20 159 1 armarego armarego PROPN eurjchem-20 159 2 , , PUNCT eurjchem-20 159 3     SPACE eurjchem-20 159 4 w. w. PROPN eurjchem-20 159 5     SPACE eurjchem-20 159 6 l. l. PROPN eurjchem-20 159 7     SPACE eurjchem-20 159 8 f. f. PROPN eurjchem-20 159 9 ; ; PUNCT eurjchem-20 159 10     SPACE eurjchem-20 159 11 perrin perrin NOUN eurjchem-20 159 12 , , PUNCT eurjchem-20 159 13     SPACE eurjchem-20 159 14 d. d. PROPN eurjchem-20 159 15     SPACE eurjchem-20 159 16 d. d. PROPN eurjchem-20 159 17     SPACE eurjchem-20 159 18 purification purification NOUN eurjchem-20 159 19     SPACE eurjchem-20 159 20 of of ADP eurjchem-20 159 21     SPACE eurjchem-20 159 22 laboratory laboratory NOUN eurjchem-20 159 23     SPACE eurjchem-20 159 24 chemicals chemical NOUN eurjchem-20 159 25 , , PUNCT eurjchem-20 159 26     SPACE eurjchem-20 159 27 4th 4th ADJ eurjchem-20 159 28     SPACE eurjchem-20 159 29 ed ed NOUN eurjchem-20 159 30 . . PROPN eurjchem-20 159 31 , , PUNCT eurjchem-20 159 32     SPACE eurjchem-20 159 33 butterworth butterworth PROPN eurjchem-20 159 34 , , PUNCT eurjchem-20 159 35     SPACE eurjchem-20 159 36 heinemann heinemann PROPN eurjchem-20 159 37 , , PUNCT eurjchem-20 159 38     SPACE eurjchem-20 159 39 oxford oxford NOUN eurjchem-20 159 40 , , PUNCT eurjchem-20 159 41     SPACE eurjchem-20 159 42 ox2 ox2 ADJ eurjchem-20 159 43     SPACE eurjchem-20 159 44 8dp 8dp NOUN eurjchem-20 159 45     SPACE eurjchem-20 159 46 1997 1997 NUM eurjchem-20 159 47 . . PUNCT eurjchem-20 159 48     SPACE eurjchem-20 160 1 [ [ X eurjchem-20 160 2 12 12 NUM eurjchem-20 160 3 ] ] PUNCT eurjchem-20 160 4 . . PUNCT eurjchem-20 161 1 murray murray PROPN eurjchem-20 161 2 , , PUNCT eurjchem-20 161 3     SPACE eurjchem-20 161 4 p. p. NOUN eurjchem-20 161 5     SPACE eurjchem-20 161 6 r. r. PROPN eurjchem-20 161 7 ; ; PUNCT eurjchem-20 161 8     SPACE eurjchem-20 161 9 baron baron NOUN eurjchem-20 161 10 , , PUNCT eurjchem-20 161 11     SPACE eurjchem-20 161 12 e. e. PROPN eurjchem-20 161 13         SPACE eurjchem-20 161 14 j. j. PROPN eurjchem-20 161 15 ; ; PUNCT eurjchem-20 161 16     SPACE eurjchem-20 161 17 pfaller pfaller NOUN eurjchem-20 161 18 , , PUNCT eurjchem-20 161 19     SPACE eurjchem-20 161 20 m. m. NOUN eurjchem-20 161 21     SPACE eurjchem-20 161 22 a. a. NOUN eurjchem-20 161 23 ; ; PUNCT eurjchem-20 161 24     SPACE eurjchem-20 161 25 tenover tenover VERB eurjchem-20 161 26 , , PUNCT eurjchem-20 161 27     SPACE eurjchem-20 161 28 f. f. PROPN eurjchem-20 161 29     SPACE eurjchem-20 161 30 c. c. PROPN eurjchem-20 161 31 ; ; PUNCT eurjchem-20 161 32     SPACE eurjchem-20 161 33 yolken yolken VERB eurjchem-20 161 34 , , PUNCT eurjchem-20 161 35     SPACE eurjchem-20 161 36 h. h. PROPN eurjchem-20 161 37     SPACE eurjchem-20 161 38 r. r. PROPN eurjchem-20 161 39     SPACE eurjchem-20 161 40 manual manual NOUN eurjchem-20 161 41     SPACE eurjchem-20 161 42 of of ADP eurjchem-20 161 43     SPACE eurjchem-20 161 44 clinical clinical ADJ eurjchem-20 161 45     SPACE eurjchem-20 161 46 microbiology microbiology NOUN eurjchem-20 161 47 , , PUNCT eurjchem-20 161 48     SPACE eurjchem-20 161 49 6th 6th ADJ eurjchem-20 161 50     SPACE eurjchem-20 161 51 ed ed NOUN eurjchem-20 161 52 . . PUNCT eurjchem-20 161 53     SPACE eurjchem-20 161 54 asm asm NOUN eurjchem-20 161 55     SPACE eurjchem-20 161 56 press press NOUN eurjchem-20 161 57 , , PUNCT eurjchem-20 161 58     SPACE eurjchem-20 161 59 washington washington PROPN eurjchem-20 161 60     SPACE eurjchem-20 161 61 dc dc PROPN eurjchem-20 161 62 , , PUNCT eurjchem-20 161 63     SPACE eurjchem-20 161 64 pp pp ADP eurjchem-20 161 65 . . PUNCT eurjchem-20 161 66     SPACE eurjchem-20 162 1 15‐18 15‐18 NUM eurjchem-20 162 2     SPACE eurjchem-20 162 3 , , PUNCT eurjchem-20 162 4     SPACE eurjchem-20 162 5 1995 1995 NUM eurjchem-20 162 6 . . PUNCT eurjchem-20 162 7     SPACE eurjchem-20 163 1 [ [ X eurjchem-20 163 2 13 13 NUM eurjchem-20 163 3 ] ] PUNCT eurjchem-20 163 4 . . PUNCT eurjchem-20 164 1 burits burit NOUN eurjchem-20 164 2 , , PUNCT eurjchem-20 164 3     SPACE eurjchem-20 164 4 m. m. NOUN eurjchem-20 164 5 ; ; PUNCT eurjchem-20 164 6     SPACE eurjchem-20 164 7 bucar bucar NOUN eurjchem-20 164 8 , , PUNCT eurjchem-20 164 9     SPACE eurjchem-20 164 10 f. f. PROPN eurjchem-20 164 11     SPACE eurjchem-20 164 12 phytother phytother PROPN eurjchem-20 164 13 . . PUNCT eurjchem-20 164 14     SPACE eurjchem-20 165 1 res re NOUN eurjchem-20 165 2 . . PUNCT eurjchem-20 165 3     SPACE eurjchem-20 165 4 2000 2000 NUM eurjchem-20 165 5 , , PUNCT eurjchem-20 165 6     SPACE eurjchem-20 165 7 14 14 NUM eurjchem-20 165 8 , , PUNCT eurjchem-20 165 9     SPACE eurjchem-20 165 10 323–328 323–328 NUM eurjchem-20 165 11 . . PUNCT eurjchem-20 165 12     SPACE eurjchem-20 166 1 [ [ X eurjchem-20 166 2 14 14 NUM eurjchem-20 166 3 ] ] PUNCT eurjchem-20 166 4 . . PUNCT eurjchem-20 167 1 kishore kishore PROPN eurjchem-20 167 2 , , PUNCT eurjchem-20 167 3         SPACE eurjchem-20 167 4 k. k. PROPN eurjchem-20 167 5     SPACE eurjchem-20 167 6 r r PROPN eurjchem-20 167 7 , , PUNCT eurjchem-20 167 8 ; ; PUNCT eurjchem-20 167 9     SPACE eurjchem-20 167 10 anil anil PROPN eurjchem-20 167 11 , , PUNCT eurjchem-20 167 12     SPACE eurjchem-20 167 13 k. k. PROPN eurjchem-20 167 14     SPACE eurjchem-20 167 15 m. m. NOUN eurjchem-20 167 16 ; ; PUNCT eurjchem-20 167 17     SPACE eurjchem-20 167 18 narayana narayana PROPN eurjchem-20 167 19 , , PUNCT eurjchem-20 167 20     SPACE eurjchem-20 167 21 r. r. PROPN eurjchem-20 167 22     SPACE eurjchem-20 167 23 m. m. NOUN eurjchem-20 167 24     SPACE eurjchem-20 167 25 v. v. PROPN eurjchem-20 167 26 ; ; PUNCT eurjchem-20 167 27     SPACE eurjchem-20 167 28 devendranath devendranath ADJ eurjchem-20 167 29 , , PUNCT eurjchem-20 167 30         SPACE eurjchem-20 167 31 r.c r.c PROPN eurjchem-20 167 32 . . PROPN eurjchem-20 167 33 ; ; PUNCT eurjchem-20 167 34     SPACE eurjchem-20 167 35 suresh suresh NOUN eurjchem-20 167 36 , , PUNCT eurjchem-20 167 37     SPACE eurjchem-20 167 38 r. r. PROPN eurjchem-20 167 39     SPACE eurjchem-20 167 40 c. c. PROPN eurjchem-20 167 41     SPACE eurjchem-20 167 42 tetrahedron tetrahedron NOUN eurjchem-20 167 43     SPACE eurjchem-20 167 44 lett lett PROPN eurjchem-20 167 45 . . PUNCT eurjchem-20 167 46     SPACE eurjchem-20 167 47 2008 2008 NUM eurjchem-20 167 48 , , PUNCT eurjchem-20 167 49     SPACE eurjchem-20 167 50 49 49 NUM eurjchem-20 167 51 , , PUNCT eurjchem-20 167 52     SPACE eurjchem-20 167 53 6337‐6340 6337‐6340 NUM eurjchem-20 167 54 . . PUNCT eurjchem-20 167 55       SPACE eurjchem-20 168 1 [ [ X eurjchem-20 168 2 15 15 NUM eurjchem-20 168 3 ] ] PUNCT eurjchem-20 168 4 . . PUNCT eurjchem-20 169 1 shirokova shirokova PROPN eurjchem-20 169 2 , , PUNCT eurjchem-20 169 3     SPACE eurjchem-20 169 4 e. e. PROPN eurjchem-20 169 5     SPACE eurjchem-20 169 6 a. a. PROPN eurjchem-20 169 7 ; ; PUNCT eurjchem-20 169 8     SPACE eurjchem-20 169 9 jasko jasko ADV eurjchem-20 169 10 , , PUNCT eurjchem-20 169 11     SPACE eurjchem-20 169 12 m. m. NOUN eurjchem-20 169 13     SPACE eurjchem-20 169 14 v. v. PROPN eurjchem-20 169 15 ; ; PUNCT eurjchem-20 169 16         SPACE eurjchem-20 169 17 khandazhinskaya khandazhinskaya NOUN eurjchem-20 169 18 , , PUNCT eurjchem-20 169 19     SPACE eurjchem-20 169 20 a. a. NOUN eurjchem-20 169 21     SPACE eurjchem-20 169 22 l. l. PROPN eurjchem-20 169 23 ; ; PUNCT eurjchem-20 169 24         SPACE eurjchem-20 169 25 ivanov ivanov PROPN eurjchem-20 169 26 , , PUNCT eurjchem-20 169 27     SPACE eurjchem-20 169 28 a. a. NOUN eurjchem-20 169 29     SPACE eurjchem-20 169 30 v. v. PROPN eurjchem-20 169 31 ; ; PUNCT eurjchem-20 169 32       SPACE eurjchem-20 169 33 yanvarev yanvarev PROPN eurjchem-20 169 34 , , PUNCT eurjchem-20 169 35         SPACE eurjchem-20 169 36 d. d. PROPN eurjchem-20 169 37     SPACE eurjchem-20 169 38 v. v. PROPN eurjchem-20 169 39 ; ; PUNCT eurjchem-20 169 40     SPACE eurjchem-20 169 41 skoblov skoblov ADJ eurjchem-20 169 42 , , PUNCT eurjchem-20 169 43     SPACE eurjchem-20 169 44 y. y. NOUN eurjchem-20 169 45     SPACE eurjchem-20 169 46 s. s. PROPN eurjchem-20 169 47 ; ; PUNCT eurjchem-20 169 48         SPACE eurjchem-20 169 49 mitkevich mitkevich NOUN eurjchem-20 169 50 , , PUNCT eurjchem-20 169 51     SPACE eurjchem-20 169 52 v. v. ADP eurjchem-20 169 53     SPACE eurjchem-20 169 54 a. a. NOUN eurjchem-20 169 55 ; ; PUNCT eurjchem-20 169 56     SPACE eurjchem-20 169 57 bocharov bocharov ADJ eurjchem-20 169 58 , , PUNCT eurjchem-20 169 59     SPACE eurjchem-20 169 60 e. e. PROPN eurjchem-20 169 61     SPACE eurjchem-20 169 62 v. v. PROPN eurjchem-20 169 63 ; ; PUNCT eurjchem-20 169 64     SPACE eurjchem-20 169 65 pronyaeva pronyaeva PROPN eurjchem-20 169 66 , , PUNCT eurjchem-20 169 67     SPACE eurjchem-20 169 68 t. t. PROPN eurjchem-20 169 69     SPACE eurjchem-20 169 70 r. r. PROPN eurjchem-20 169 71 ; ; PUNCT eurjchem-20 169 72         SPACE eurjchem-20 169 73 fedyuk fedyuk NOUN eurjchem-20 169 74 , , PUNCT eurjchem-20 169 75     SPACE eurjchem-20 169 76 n. n. NOUN eurjchem-20 169 77     SPACE eurjchem-20 169 78 v. v. PROPN eurjchem-20 169 79 ; ; PUNCT eurjchem-20 169 80     SPACE eurjchem-20 169 81 kukhanova kukhanova PROPN eurjchem-20 169 82 , , PUNCT eurjchem-20 169 83     SPACE eurjchem-20 169 84 m. m. NOUN eurjchem-20 169 85     SPACE eurjchem-20 169 86 k. k. PROPN eurjchem-20 169 87 ; ; PUNCT eurjchem-20 169 88     SPACE eurjchem-20 169 89 pokrovsky pokrovsky ADJ eurjchem-20 169 90 , , PUNCT eurjchem-20 169 91     SPACE eurjchem-20 169 92 a. a. NOUN eurjchem-20 169 93     SPACE eurjchem-20 169 94 g. g. PROPN eurjchem-20 169 95     SPACE eurjchem-20 169 96 j. j. PROPN eurjchem-20 169 97     SPACE eurjchem-20 169 98 med med PROPN eurjchem-20 169 99 . . PUNCT eurjchem-20 169 100     SPACE eurjchem-20 169 101 chem chem NOUN eurjchem-20 169 102 . . PUNCT eurjchem-20 169 103     SPACE eurjchem-20 170 1 2004 2004 NUM eurjchem-20 170 2 , , PUNCT eurjchem-20 170 3     SPACE eurjchem-20 170 4 47 47 NUM eurjchem-20 170 5 , , PUNCT eurjchem-20 170 6     SPACE eurjchem-20 170 7 3606–3614 3606–3614 NUM eurjchem-20 170 8 . . PUNCT eurjchem-20 170 9     SPACE eurjchem-20 171 1 [ [ X eurjchem-20 171 2 16 16 NUM eurjchem-20 171 3 ] ] PUNCT eurjchem-20 171 4 . . PUNCT eurjchem-20 172 1 kim kim PROPN eurjchem-20 172 2 , , PUNCT eurjchem-20 172 3     SPACE eurjchem-20 172 4 j. j. PROPN eurjchem-20 172 5 ; ; PUNCT eurjchem-20 172 6     SPACE eurjchem-20 172 7 chou chou NOUN eurjchem-20 172 8 , , PUNCT eurjchem-20 172 9     SPACE eurjchem-20 172 10 t. t. PROPN eurjchem-20 172 11     SPACE eurjchem-20 172 12 f. f. PROPN eurjchem-20 172 13 ; ; PUNCT eurjchem-20 172 14     SPACE eurjchem-20 172 15 griesgraber griesgraber PROPN eurjchem-20 172 16 , , PUNCT eurjchem-20 172 17     SPACE eurjchem-20 172 18 g. g. PROPN eurjchem-20 172 19     SPACE eurjchem-20 172 20 w. w. PROPN eurjchem-20 172 21 ; ; PUNCT eurjchem-20 172 22     SPACE eurjchem-20 172 23 wagner wagner PROPN eurjchem-20 172 24 , , PUNCT eurjchem-20 172 25     SPACE eurjchem-20 172 26 c. c. PROPN eurjchem-20 172 27     SPACE eurjchem-20 172 28 r. r. PROPN eurjchem-20 172 29     SPACE eurjchem-20 172 30 mol mol PROPN eurjchem-20 172 31 . . PROPN eurjchem-20 172 32     SPACE eurjchem-20 172 33 pharmaceutics pharmaceutic NOUN eurjchem-20 172 34     SPACE eurjchem-20 172 35 2004 2004 NUM eurjchem-20 172 36 , , PUNCT eurjchem-20 172 37     SPACE eurjchem-20 172 38 1 1 NUM eurjchem-20 172 39 , , PUNCT eurjchem-20 172 40     SPACE eurjchem-20 172 41 102‐111 102‐111 PROPN eurjchem-20 172 42 . . PUNCT eurjchem-20 172 43       SPACE eurjchem-20 173 1 [ [ X eurjchem-20 173 2 17 17 NUM eurjchem-20 173 3 ] ] PUNCT eurjchem-20 173 4 . . PUNCT eurjchem-20 174 1 mcguigan mcguigan PROPN eurjchem-20 174 2 , , PUNCT eurjchem-20 174 3     SPACE eurjchem-20 174 4 c. c. NOUN eurjchem-20 174 5 ; ; PUNCT eurjchem-20 174 6     SPACE eurjchem-20 174 7 cahard cahard NOUN eurjchem-20 174 8 , , PUNCT eurjchem-20 174 9     SPACE eurjchem-20 174 10 d. d. PROPN eurjchem-20 174 11 ; ; PUNCT eurjchem-20 174 12     SPACE eurjchem-20 174 13 sheeka sheeka PROPN eurjchem-20 174 14 , , PUNCT eurjchem-20 174 15     SPACE eurjchem-20 174 16 h.m h.m PROPN eurjchem-20 174 17 . . PROPN eurjchem-20 174 18 ; ; PUNCT eurjchem-20 174 19     SPACE eurjchem-20 174 20 clercq clercq NOUN eurjchem-20 174 21 , , PUNCT eurjchem-20 174 22     SPACE eurjchem-20 174 23 e.d e.d PROPN eurjchem-20 174 24 . . PROPN eurjchem-20 174 25 ; ; PUNCT eurjchem-20 174 26     SPACE eurjchem-20 174 27 balzarini balzarini NOUN eurjchem-20 174 28 , , PUNCT eurjchem-20 174 29     SPACE eurjchem-20 174 30 j. j. PROPN eurjchem-20 174 31       SPACE eurjchem-20 174 32 j. j. PROPN eurjchem-20 174 33     SPACE eurjchem-20 174 34 med med PROPN eurjchem-20 174 35 . . PUNCT eurjchem-20 174 36     SPACE eurjchem-20 174 37 chem chem NOUN eurjchem-20 174 38 . . PUNCT eurjchem-20 174 39     SPACE eurjchem-20 174 40 1996 1996 NUM eurjchem-20 174 41 , , PUNCT eurjchem-20 174 42     SPACE eurjchem-20 174 43 39 39 NUM eurjchem-20 174 44 , , PUNCT eurjchem-20 174 45     SPACE eurjchem-20 174 46 1748‐1753 1748‐1753 NUM eurjchem-20 174 47 . . PUNCT eurjchem-20 174 48     SPACE eurjchem-20 175 1 [ [ X eurjchem-20 175 2 18 18 NUM eurjchem-20 175 3 ] ] PUNCT eurjchem-20 175 4 . . PUNCT eurjchem-20 176 1 koteswara koteswara PROPN eurjchem-20 176 2     SPACE eurjchem-20 176 3 rao rao PROPN eurjchem-20 176 4 , , PUNCT eurjchem-20 176 5     SPACE eurjchem-20 176 6 v. v. PROPN eurjchem-20 176 7 ; ; PUNCT eurjchem-20 176 8     SPACE eurjchem-20 176 9 janardhan janardhan PROPN eurjchem-20 176 10     SPACE eurjchem-20 176 11 rao rao PROPN eurjchem-20 176 12 , , PUNCT eurjchem-20 176 13     SPACE eurjchem-20 176 14 a. a. NOUN eurjchem-20 176 15 ; ; PUNCT eurjchem-20 176 16     SPACE eurjchem-20 176 17 subba subba NOUN eurjchem-20 176 18     SPACE eurjchem-20 176 19 reddy reddy NOUN eurjchem-20 176 20 , , PUNCT eurjchem-20 176 21     SPACE eurjchem-20 176 22 s. s. PROPN eurjchem-20 176 23 ; ; PUNCT eurjchem-20 176 24     SPACE eurjchem-20 176 25 naga naga NOUN eurjchem-20 176 26     SPACE eurjchem-20 176 27 raju raju PROPN eurjchem-20 176 28 , , PUNCT eurjchem-20 176 29     SPACE eurjchem-20 176 30 c. c. NOUN eurjchem-20 176 31 ; ; PUNCT eurjchem-20 176 32     SPACE eurjchem-20 176 33 visweswara visweswara PROPN eurjchem-20 176 34     SPACE eurjchem-20 176 35 rao rao PROPN eurjchem-20 176 36 , , PUNCT eurjchem-20 176 37     SPACE eurjchem-20 176 38 p. p. NOUN eurjchem-20 176 39 ; ; PUNCT eurjchem-20 176 40     SPACE eurjchem-20 176 41 ghosh ghosh PROPN eurjchem-20 176 42 . . PUNCT eurjchem-20 176 43     SPACE eurjchem-20 177 1 s. s. PROPN eurjchem-20 177 2     SPACE eurjchem-20 177 3 k. k. PROPN eurjchem-20 177 4         SPACE eurjchem-20 177 5 eur eur PROPN eurjchem-20 177 6 . . PUNCT eurjchem-20 177 7     SPACE eurjchem-20 177 8 j. j. PROPN eurjchem-20 177 9         SPACE eurjchem-20 177 10 med med PROPN eurjchem-20 177 11 . . PUNCT eurjchem-20 177 12     SPACE eurjchem-20 177 13 chem chem NOUN eurjchem-20 177 14 . . PUNCT eurjchem-20 177 15     SPACE eurjchem-20 178 1 2010 2010 NUM eurjchem-20 178 2 , , PUNCT eurjchem-20 178 3     SPACE eurjchem-20 178 4 45 45 NUM eurjchem-20 178 5 , , PUNCT eurjchem-20 178 6     SPACE eurjchem-20 178 7 203 203 NUM eurjchem-20 178 8 – – PUNCT eurjchem-20 178 9 209 209 NUM eurjchem-20 178 10 . . PUNCT eurjchem-20 178 11         SPACE