id	sid	tid	token	lemma	pos
eurjchem-2064	1	1	the	the	DET
eurjchem-2064	1	2	synthesis	synthesis	NOUN
eurjchem-2064	1	3	and	and	CCONJ
eurjchem-2064	1	4	crystallographic	crystallographic	ADJ
eurjchem-2064	1	5	characterization	characterization	NOUN
eurjchem-2064	1	6	of	of	ADP
eurjchem-2064	1	7	4	4	NUM
eurjchem-2064	1	8	-	-	PUNCT
eurjchem-2064	1	9	methylbenzenesulfonamide	methylbenzenesulfonamide	NOUN
eurjchem-2064	1	10	derivatives	derivative	NOUN
eurjchem-2064	1	11	european	european	PROPN
eurjchem-2064	1	12	journal	journal	PROPN
eurjchem-2064	1	13	of	of	ADP
eurjchem-2064	1	14	chemistry	chemistry	NOUN
eurjchem-2064	1	15	12	12	NUM
eurjchem-2064	1	16	(	(	PUNCT
eurjchem-2064	1	17	2	2	NUM
eurjchem-2064	1	18	)	)	PUNCT
eurjchem-2064	1	19	(	(	PUNCT
eurjchem-2064	1	20	2021	2021	NUM
eurjchem-2064	1	21	)	)	PUNCT
eurjchem-2064	1	22	109	109	NUM
eurjchem-2064	1	23	-	-	SYM
eurjchem-2064	1	24	116	116	NUM
eurjchem-2064	1	25	european	european	ADJ
eurjchem-2064	1	26	journal	journal	PROPN
eurjchem-2064	1	27	of	of	ADP
eurjchem-2064	1	28	chemistry	chemistry	NOUN
eurjchem-2064	1	29	issn	issn	VERB
eurjchem-2064	1	30	2153	2153	NUM
eurjchem-2064	1	31	-	-	SYM
eurjchem-2064	1	32	2249	2249	NUM
eurjchem-2064	1	33	(	(	PUNCT
eurjchem-2064	1	34	print	print	NOUN
eurjchem-2064	1	35	)	)	PUNCT
eurjchem-2064	1	36	/	/	PUNCT
eurjchem-2064	1	37	issn	issn	PROPN
eurjchem-2064	1	38	2153	2153	NUM
eurjchem-2064	1	39	-	-	SYM
eurjchem-2064	1	40	2257	2257	NUM
eurjchem-2064	1	41	(	(	PUNCT
eurjchem-2064	1	42	online	online	ADJ
eurjchem-2064	1	43	)	)	PUNCT
eurjchem-2064	1	44	–	–	PUNCT
eurjchem-2064	2	1	copyright	copyright	NOUN
eurjchem-2064	2	2	©	©	PROPN
eurjchem-2064	2	3	2021	2021	NUM
eurjchem-2064	2	4	the	the	DET
eurjchem-2064	2	5	authors	author	NOUN
eurjchem-2064	2	6	–	–	PUNCT
eurjchem-2064	2	7	atlanta	atlanta	PROPN
eurjchem-2064	2	8	publishing	publishing	PROPN
eurjchem-2064	2	9	house	house	PROPN
eurjchem-2064	2	10	llc	llc	PROPN
eurjchem-2064	2	11	–	–	PUNCT
eurjchem-2064	2	12	printed	print	VERB
eurjchem-2064	2	13	in	in	ADP
eurjchem-2064	2	14	the	the	DET
eurjchem-2064	2	15	usa	usa	PROPN
eurjchem-2064	2	16	.	.	PUNCT
eurjchem-2064	3	1	this	this	DET
eurjchem-2064	3	2	work	work	NOUN
eurjchem-2064	3	3	is	be	AUX
eurjchem-2064	3	4	published	publish	VERB
eurjchem-2064	3	5	and	and	CCONJ
eurjchem-2064	3	6	licensed	license	VERB
eurjchem-2064	3	7	by	by	ADP
eurjchem-2064	3	8	atlanta	atlanta	PROPN
eurjchem-2064	3	9	publishing	publishing	PROPN
eurjchem-2064	3	10	house	house	PROPN
eurjchem-2064	3	11	llc	llc	PROPN
eurjchem-2064	3	12	–	–	PUNCT
eurjchem-2064	3	13	cc	cc	PROPN
eurjchem-2064	3	14	by	by	ADP
eurjchem-2064	3	15	nc	nc	PROPN
eurjchem-2064	3	16	–	–	PUNCT
eurjchem-2064	3	17	some	some	DET
eurjchem-2064	3	18	rights	right	NOUN
eurjchem-2064	3	19	reserved	reserve	VERB
eurjchem-2064	3	20	.	.	PUNCT
eurjchem-2064	4	1	https://dx.doi.org/10.5155/eurjchem.12.2.109-116.2064	https://dx.doi.org/10.5155/eurjchem.12.2.109-116.2064	PROPN
eurjchem-2064	4	2	european	european	PROPN
eurjchem-2064	4	3	journal	journal	PROPN
eurjchem-2064	4	4	of	of	ADP
eurjchem-2064	4	5	chemistry	chemistry	NOUN
eurjchem-2064	4	6	view	view	NOUN
eurjchem-2064	4	7	journal	journal	PROPN
eurjchem-2064	4	8	online	online	PROPN
eurjchem-2064	4	9	view	view	NOUN
eurjchem-2064	4	10	article	article	NOUN
eurjchem-2064	4	11	online	online	VERB
eurjchem-2064	4	12	the	the	DET
eurjchem-2064	4	13	synthesis	synthesis	NOUN
eurjchem-2064	4	14	and	and	CCONJ
eurjchem-2064	4	15	crystallographic	crystallographic	ADJ
eurjchem-2064	4	16	characterization	characterization	NOUN
eurjchem-2064	4	17	of	of	ADP
eurjchem-2064	4	18	4	4	NUM
eurjchem-2064	4	19	-	-	PUNCT
eurjchem-2064	4	20	methylbenzenesulfonamide	methylbenzenesulfonamide	NOUN
eurjchem-2064	4	21	derivatives	derivative	NOUN
eurjchem-2064	4	22	brock	brock	PROPN
eurjchem-2064	4	23	anton	anton	PROPN
eurjchem-2064	4	24	stenfors	stenfor	NOUN
eurjchem-2064	4	25	and	and	CCONJ
eurjchem-2064	4	26	felix	felix	PROPN
eurjchem-2064	4	27	nyuangem	nyuangem	PROPN
eurjchem-2064	4	28	ngassa	ngassa	PROPN
eurjchem-2064	4	29	*	*	PUNCT
eurjchem-2064	4	30	department	department	NOUN
eurjchem-2064	4	31	of	of	ADP
eurjchem-2064	4	32	chemistry	chemistry	NOUN
eurjchem-2064	4	33	,	,	PUNCT
eurjchem-2064	4	34	grand	grand	ADJ
eurjchem-2064	4	35	valley	valley	PROPN
eurjchem-2064	4	36	state	state	PROPN
eurjchem-2064	4	37	university	university	PROPN
eurjchem-2064	4	38	,	,	PUNCT
eurjchem-2064	4	39	1	1	NUM
eurjchem-2064	4	40	campus	campus	NOUN
eurjchem-2064	4	41	drive	drive	NOUN
eurjchem-2064	4	42	,	,	PUNCT
eurjchem-2064	4	43	allendale	allendale	PROPN
eurjchem-2064	4	44	,	,	PUNCT
eurjchem-2064	4	45	mi	mi	PROPN
eurjchem-2064	4	46	49401	49401	NUM
eurjchem-2064	4	47	,	,	PUNCT
eurjchem-2064	4	48	usa	usa	PROPN
eurjchem-2064	4	49	stenforb@mail.gvsu.edu	stenforb@mail.gvsu.edu	PROPN
eurjchem-2064	4	50	(	(	PUNCT
eurjchem-2064	4	51	b.a.s	b.a.s	PROPN
eurjchem-2064	4	52	.	.	PUNCT
eurjchem-2064	4	53	)	)	PUNCT
eurjchem-2064	4	54	,	,	PUNCT
eurjchem-2064	4	55	ngassaf@gvsu.edu	ngassaf@gvsu.edu	PROPN
eurjchem-2064	4	56	(	(	PUNCT
eurjchem-2064	4	57	f.n.n	f.n.n	PROPN
eurjchem-2064	4	58	.	.	PUNCT
eurjchem-2064	4	59	)	)	PUNCT
eurjchem-2064	5	1	*	*	PUNCT
eurjchem-2064	5	2	corresponding	correspond	VERB
eurjchem-2064	5	3	author	author	NOUN
eurjchem-2064	5	4	at	at	ADP
eurjchem-2064	5	5	:	:	PUNCT
eurjchem-2064	5	6	department	department	NOUN
eurjchem-2064	5	7	of	of	ADP
eurjchem-2064	5	8	chemistry	chemistry	NOUN
eurjchem-2064	5	9	,	,	PUNCT
eurjchem-2064	5	10	grand	grand	ADJ
eurjchem-2064	5	11	valley	valley	PROPN
eurjchem-2064	5	12	state	state	PROPN
eurjchem-2064	5	13	university	university	PROPN
eurjchem-2064	5	14	,	,	PUNCT
eurjchem-2064	5	15	1	1	NUM
eurjchem-2064	5	16	campus	campus	NOUN
eurjchem-2064	5	17	drive	drive	NOUN
eurjchem-2064	5	18	,	,	PUNCT
eurjchem-2064	5	19	allendale	allendale	PROPN
eurjchem-2064	5	20	,	,	PUNCT
eurjchem-2064	5	21	mi	mi	PROPN
eurjchem-2064	5	22	49401	49401	NUM
eurjchem-2064	5	23	,	,	PUNCT
eurjchem-2064	5	24	usa	usa	PROPN
eurjchem-2064	5	25	.	.	PROPN
eurjchem-2064	5	26	e	e	X
eurjchem-2064	5	27	-	-	NOUN
eurjchem-2064	5	28	mail	mail	NOUN
eurjchem-2064	5	29	:	:	PUNCT
eurjchem-2064	5	30	ngassaf@gvsu.edu	ngassaf@gvsu.edu	PROPN
eurjchem-2064	5	31	(	(	PUNCT
eurjchem-2064	5	32	f.n	f.n	PROPN
eurjchem-2064	5	33	.	.	NOUN
eurjchem-2064	5	34	ngassa	ngassa	NOUN
eurjchem-2064	5	35	)	)	PUNCT
eurjchem-2064	5	36	.	.	PUNCT
eurjchem-2064	6	1	10.5155	10.5155	NUM
eurjchem-2064	6	2	/	/	SYM
eurjchem-2064	6	3	eurjchem.12.2.109	eurjchem.12.2.109	NUM
eurjchem-2064	6	4	-	-	PUNCT
eurjchem-2064	6	5	116.2064	116.2064	NUM
eurjchem-2064	6	6	received	receive	VERB
eurjchem-2064	6	7	:	:	PUNCT
eurjchem-2064	6	8	09	09	NUM
eurjchem-2064	6	9	january	january	NOUN
eurjchem-2064	6	10	2021	2021	NUM
eurjchem-2064	6	11	received	receive	VERB
eurjchem-2064	6	12	in	in	ADP
eurjchem-2064	6	13	revised	revise	VERB
eurjchem-2064	6	14	form	form	NOUN
eurjchem-2064	6	15	:	:	PUNCT
eurjchem-2064	6	16	16	16	NUM
eurjchem-2064	6	17	march	march	NOUN
eurjchem-2064	6	18	2021	2021	NUM
eurjchem-2064	6	19	accepted	accept	VERB
eurjchem-2064	6	20	:	:	PUNCT
eurjchem-2064	6	21	28	28	NUM
eurjchem-2064	6	22	march	march	NOUN
eurjchem-2064	6	23	2021	2021	NUM
eurjchem-2064	6	24	published	publish	VERB
eurjchem-2064	6	25	online	online	ADV
eurjchem-2064	6	26	:	:	PUNCT
eurjchem-2064	6	27	30	30	NUM
eurjchem-2064	6	28	june	june	PROPN
eurjchem-2064	6	29	2021	2021	NUM
eurjchem-2064	6	30	printed	print	VERB
eurjchem-2064	6	31	:	:	PUNCT
eurjchem-2064	6	32	30	30	NUM
eurjchem-2064	6	33	june	june	PROPN
eurjchem-2064	6	34	2021	2021	NUM
eurjchem-2064	6	35	the	the	DET
eurjchem-2064	6	36	sulfonamide	sulfonamide	ADJ
eurjchem-2064	6	37	moiety	moiety	NOUN
eurjchem-2064	6	38	is	be	AUX
eurjchem-2064	6	39	present	present	ADJ
eurjchem-2064	6	40	among	among	ADP
eurjchem-2064	6	41	a	a	DET
eurjchem-2064	6	42	variety	variety	NOUN
eurjchem-2064	6	43	of	of	ADP
eurjchem-2064	6	44	biologically	biologically	ADV
eurjchem-2064	6	45	significant	significant	ADJ
eurjchem-2064	6	46	compounds	compound	NOUN
eurjchem-2064	6	47	.	.	PUNCT
eurjchem-2064	7	1	a	a	DET
eurjchem-2064	7	2	facile	facile	ADJ
eurjchem-2064	7	3	synthesis	synthesis	NOUN
eurjchem-2064	7	4	is	be	AUX
eurjchem-2064	7	5	necessary	necessary	ADJ
eurjchem-2064	7	6	to	to	PART
eurjchem-2064	7	7	produce	produce	VERB
eurjchem-2064	7	8	a	a	DET
eurjchem-2064	7	9	variety	variety	NOUN
eurjchem-2064	7	10	of	of	ADP
eurjchem-2064	7	11	sulfonamides	sulfonamide	NOUN
eurjchem-2064	7	12	with	with	ADP
eurjchem-2064	7	13	the	the	DET
eurjchem-2064	7	14	potential	potential	NOUN
eurjchem-2064	7	15	to	to	PART
eurjchem-2064	7	16	improve	improve	VERB
eurjchem-2064	7	17	human	human	ADJ
eurjchem-2064	7	18	health	health	NOUN
eurjchem-2064	7	19	.	.	PUNCT
eurjchem-2064	8	1	herein	herein	NOUN
eurjchem-2064	8	2	,	,	PUNCT
eurjchem-2064	8	3	we	we	PRON
eurjchem-2064	8	4	report	report	VERB
eurjchem-2064	8	5	a	a	DET
eurjchem-2064	8	6	facile	facile	ADJ
eurjchem-2064	8	7	methodology	methodology	NOUN
eurjchem-2064	8	8	for	for	ADP
eurjchem-2064	8	9	the	the	DET
eurjchem-2064	8	10	synthesis	synthesis	NOUN
eurjchem-2064	8	11	of	of	ADP
eurjchem-2064	8	12	4methylbenzenesulfonamides	4methylbenzenesulfonamides	NUM
eurjchem-2064	8	13	,	,	PUNCT
eurjchem-2064	8	14	amenable	amenable	ADJ
eurjchem-2064	8	15	to	to	ADP
eurjchem-2064	8	16	a	a	DET
eurjchem-2064	8	17	broad	broad	ADJ
eurjchem-2064	8	18	range	range	NOUN
eurjchem-2064	8	19	of	of	ADP
eurjchem-2064	8	20	nitrogen	nitrogen	NOUN
eurjchem-2064	8	21	nucleophiles	nucleophile	NOUN
eurjchem-2064	8	22	.	.	PUNCT
eurjchem-2064	9	1	implementing	implement	VERB
eurjchem-2064	9	2	a	a	DET
eurjchem-2064	9	3	semi	semi	ADJ
eurjchem-2064	9	4	-	-	ADJ
eurjchem-2064	9	5	miscible	miscible	ADJ
eurjchem-2064	9	6	biphasic	biphasic	ADJ
eurjchem-2064	9	7	solvent	solvent	NOUN
eurjchem-2064	9	8	system	system	NOUN
eurjchem-2064	9	9	resulted	result	VERB
eurjchem-2064	9	10	in	in	ADP
eurjchem-2064	9	11	higher	high	ADJ
eurjchem-2064	9	12	yields	yield	NOUN
eurjchem-2064	9	13	,	,	PUNCT
eurjchem-2064	9	14	decreased	decrease	VERB
eurjchem-2064	9	15	reaction	reaction	NOUN
eurjchem-2064	9	16	times	time	NOUN
eurjchem-2064	9	17	,	,	PUNCT
eurjchem-2064	9	18	and	and	CCONJ
eurjchem-2064	9	19	a	a	DET
eurjchem-2064	9	20	simplified	simplified	ADJ
eurjchem-2064	9	21	workup	workup	NOUN
eurjchem-2064	9	22	over	over	ADP
eurjchem-2064	9	23	preliminary	preliminary	ADJ
eurjchem-2064	9	24	methods	method	NOUN
eurjchem-2064	9	25	.	.	PUNCT
eurjchem-2064	10	1	additionally	additionally	ADV
eurjchem-2064	10	2	,	,	PUNCT
eurjchem-2064	10	3	the	the	DET
eurjchem-2064	10	4	crystal	crystal	NOUN
eurjchem-2064	10	5	structures	structure	NOUN
eurjchem-2064	10	6	of	of	ADP
eurjchem-2064	10	7	five	five	NUM
eurjchem-2064	10	8	novel	novel	ADJ
eurjchem-2064	10	9	sulfonamide	sulfonamide	NOUN
eurjchem-2064	10	10	compounds	compound	NOUN
eurjchem-2064	10	11	and	and	CCONJ
eurjchem-2064	10	12	two	two	NUM
eurjchem-2064	10	13	polymorphs	polymorph	NOUN
eurjchem-2064	10	14	,	,	PUNCT
eurjchem-2064	10	15	have	have	AUX
eurjchem-2064	10	16	been	be	AUX
eurjchem-2064	10	17	determined	determine	VERB
eurjchem-2064	10	18	by	by	ADP
eurjchem-2064	10	19	x	x	NOUN
eurjchem-2064	10	20	-	-	NOUN
eurjchem-2064	10	21	ray	ray	NOUN
eurjchem-2064	10	22	diffraction	diffraction	NOUN
eurjchem-2064	10	23	.	.	PUNCT
eurjchem-2064	11	1	results	result	NOUN
eurjchem-2064	11	2	obtained	obtain	VERB
eurjchem-2064	11	3	through	through	ADP
eurjchem-2064	11	4	spectroscopic	spectroscopic	ADJ
eurjchem-2064	11	5	characterization	characterization	NOUN
eurjchem-2064	11	6	support	support	NOUN
eurjchem-2064	11	7	the	the	DET
eurjchem-2064	11	8	successful	successful	ADJ
eurjchem-2064	11	9	formation	formation	NOUN
eurjchem-2064	11	10	of	of	ADP
eurjchem-2064	11	11	the	the	DET
eurjchem-2064	11	12	desired	desire	VERB
eurjchem-2064	11	13	4	4	NUM
eurjchem-2064	11	14	-	-	PUNCT
eurjchem-2064	11	15	methylbenzenesulfonamides	methylbenzenesulfonamide	NOUN
eurjchem-2064	11	16	.	.	PUNCT
eurjchem-2064	12	1	tosylation	tosylation	NOUN
eurjchem-2064	12	2	sulfa	sulfa	NOUN
eurjchem-2064	12	3	drugs	drug	NOUN
eurjchem-2064	12	4	methodology	methodology	NOUN
eurjchem-2064	12	5	sulfonamides	sulfonamide	VERB
eurjchem-2064	12	6	crystal	crystal	NOUN
eurjchem-2064	12	7	structures	structure	NOUN
eurjchem-2064	12	8	packing	pack	VERB
eurjchem-2064	12	9	polymorph	polymorph	NOUN
eurjchem-2064	12	10	cite	cite	VERB
eurjchem-2064	12	11	this	this	PRON
eurjchem-2064	12	12	:	:	PUNCT
eurjchem-2064	12	13	eur	eur	PROPN
eurjchem-2064	12	14	.	.	PUNCT
eurjchem-2064	13	1	j.	j.	PROPN
eurjchem-2064	13	2	chem	chem	PROPN
eurjchem-2064	13	3	.	.	PUNCT
eurjchem-2064	14	1	2021	2021	NUM
eurjchem-2064	14	2	,	,	PUNCT
eurjchem-2064	14	3	12(2	12(2	NUM
eurjchem-2064	14	4	)	)	PUNCT
eurjchem-2064	14	5	,	,	PUNCT
eurjchem-2064	14	6	109	109	NUM
eurjchem-2064	14	7	-	-	SYM
eurjchem-2064	14	8	116	116	NUM
eurjchem-2064	14	9	journal	journal	NOUN
eurjchem-2064	14	10	website	website	NOUN
eurjchem-2064	14	11	:	:	PUNCT
eurjchem-2064	14	12	www.eurjchem.com	www.eurjchem.com	X
eurjchem-2064	14	13	1	1	X
eurjchem-2064	14	14	.	.	PUNCT
eurjchem-2064	14	15	introduction	introduction	NOUN
eurjchem-2064	14	16	sulfonamides	sulfonamide	NOUN
eurjchem-2064	14	17	,	,	PUNCT
eurjchem-2064	14	18	commonly	commonly	ADV
eurjchem-2064	14	19	referred	refer	VERB
eurjchem-2064	14	20	to	to	ADP
eurjchem-2064	14	21	as	as	ADP
eurjchem-2064	14	22	sulfa	sulfa	NOUN
eurjchem-2064	14	23	drugs	drug	NOUN
eurjchem-2064	14	24	,	,	PUNCT
eurjchem-2064	14	25	are	be	AUX
eurjchem-2064	14	26	biologically	biologically	ADV
eurjchem-2064	14	27	significant	significant	ADJ
eurjchem-2064	14	28	compounds	compound	NOUN
eurjchem-2064	14	29	with	with	ADP
eurjchem-2064	14	30	diverse	diverse	ADJ
eurjchem-2064	14	31	biological	biological	ADJ
eurjchem-2064	14	32	properties	property	NOUN
eurjchem-2064	14	33	that	that	PRON
eurjchem-2064	14	34	continue	continue	VERB
eurjchem-2064	14	35	to	to	PART
eurjchem-2064	14	36	show	show	VERB
eurjchem-2064	14	37	promise	promise	NOUN
eurjchem-2064	14	38	in	in	ADP
eurjchem-2064	14	39	modern	modern	ADJ
eurjchem-2064	14	40	-	-	PUNCT
eurjchem-2064	14	41	day	day	NOUN
eurjchem-2064	14	42	therapeutics	therapeutic	NOUN
eurjchem-2064	14	43	.	.	PUNCT
eurjchem-2064	15	1	the	the	DET
eurjchem-2064	15	2	discovery	discovery	NOUN
eurjchem-2064	15	3	of	of	ADP
eurjchem-2064	15	4	sulfonamide	sulfonamide	NOUN
eurjchem-2064	15	5	agents	agent	NOUN
eurjchem-2064	15	6	began	begin	VERB
eurjchem-2064	15	7	with	with	ADP
eurjchem-2064	15	8	the	the	DET
eurjchem-2064	15	9	synthesis	synthesis	NOUN
eurjchem-2064	15	10	of	of	ADP
eurjchem-2064	15	11	sulfanilamide	sulfanilamide	NOUN
eurjchem-2064	15	12	in	in	ADP
eurjchem-2064	15	13	1908	1908	NUM
eurjchem-2064	15	14	by	by	ADP
eurjchem-2064	15	15	gelmo	gelmo	NOUN
eurjchem-2064	15	16	et	et	PROPN
eurjchem-2064	15	17	al	al	PROPN
eurjchem-2064	15	18	.	.	PUNCT
eurjchem-2064	16	1	[	[	X
eurjchem-2064	16	2	1	1	NUM
eurjchem-2064	16	3	]	]	PUNCT
eurjchem-2064	16	4	.	.	PUNCT
eurjchem-2064	17	1	a	a	DET
eurjchem-2064	17	2	prodrug	prodrug	NOUN
eurjchem-2064	17	3	of	of	ADP
eurjchem-2064	17	4	sulfanilamide	sulfanilamide	NOUN
eurjchem-2064	17	5	,	,	PUNCT
eurjchem-2064	17	6	prontosil	prontosil	NOUN
eurjchem-2064	17	7	,	,	PUNCT
eurjchem-2064	17	8	synthesized	synthesize	VERB
eurjchem-2064	17	9	by	by	ADP
eurjchem-2064	17	10	domagk	domagk	PROPN
eurjchem-2064	17	11	et	et	PROPN
eurjchem-2064	17	12	al	al	PROPN
eurjchem-2064	17	13	.	.	PROPN
eurjchem-2064	18	1	in	in	ADP
eurjchem-2064	18	2	1935	1935	NUM
eurjchem-2064	18	3	,	,	PUNCT
eurjchem-2064	18	4	became	become	VERB
eurjchem-2064	18	5	the	the	DET
eurjchem-2064	18	6	first	first	ADJ
eurjchem-2064	18	7	effective	effective	ADJ
eurjchem-2064	18	8	antibacterial	antibacterial	ADJ
eurjchem-2064	18	9	agent	agent	NOUN
eurjchem-2064	18	10	[	[	X
eurjchem-2064	18	11	2	2	NUM
eurjchem-2064	18	12	]	]	PUNCT
eurjchem-2064	18	13	.	.	PUNCT
eurjchem-2064	19	1	these	these	DET
eurjchem-2064	19	2	findings	finding	NOUN
eurjchem-2064	19	3	led	lead	VERB
eurjchem-2064	19	4	to	to	ADP
eurjchem-2064	19	5	the	the	DET
eurjchem-2064	19	6	production	production	NOUN
eurjchem-2064	19	7	of	of	ADP
eurjchem-2064	19	8	numerous	numerous	ADJ
eurjchem-2064	19	9	sulfonamide	sulfonamide	ADJ
eurjchem-2064	19	10	drugs	drug	NOUN
eurjchem-2064	19	11	.	.	PUNCT
eurjchem-2064	20	1	in	in	ADP
eurjchem-2064	20	2	1937	1937	NUM
eurjchem-2064	20	3	,	,	PUNCT
eurjchem-2064	20	4	the	the	DET
eurjchem-2064	20	5	synthesis	synthesis	NOUN
eurjchem-2064	20	6	of	of	ADP
eurjchem-2064	20	7	sulfapyridine	sulfapyridine	NOUN
eurjchem-2064	20	8	,	,	PUNCT
eurjchem-2064	20	9	better	well	ADV
eurjchem-2064	20	10	known	know	VERB
eurjchem-2064	20	11	as	as	ADP
eurjchem-2064	20	12	m&b	m&b	PROPN
eurjchem-2064	20	13	693	693	NUM
eurjchem-2064	20	14	,	,	PUNCT
eurjchem-2064	20	15	became	become	VERB
eurjchem-2064	20	16	the	the	DET
eurjchem-2064	20	17	first	first	ADJ
eurjchem-2064	20	18	known	know	VERB
eurjchem-2064	20	19	treatment	treatment	NOUN
eurjchem-2064	20	20	for	for	ADP
eurjchem-2064	20	21	pneumonia	pneumonia	NOUN
eurjchem-2064	20	22	[	[	X
eurjchem-2064	20	23	3,4	3,4	NUM
eurjchem-2064	20	24	]	]	PUNCT
eurjchem-2064	20	25	.	.	PUNCT
eurjchem-2064	21	1	in	in	ADP
eurjchem-2064	21	2	the	the	DET
eurjchem-2064	21	3	years	year	NOUN
eurjchem-2064	21	4	preceding	precede	VERB
eurjchem-2064	21	5	,	,	PUNCT
eurjchem-2064	21	6	sulfonamides	sulfonamide	NOUN
eurjchem-2064	21	7	have	have	AUX
eurjchem-2064	21	8	exhibited	exhibit	VERB
eurjchem-2064	21	9	antibacterial	antibacterial	ADJ
eurjchem-2064	21	10	,	,	PUNCT
eurjchem-2064	21	11	antiviral	antiviral	NOUN
eurjchem-2064	21	12	,	,	PUNCT
eurjchem-2064	21	13	antimalarial	antimalarial	NOUN
eurjchem-2064	21	14	,	,	PUNCT
eurjchem-2064	21	15	antifungal	antifungal	ADJ
eurjchem-2064	21	16	,	,	PUNCT
eurjchem-2064	21	17	anticancer	anticancer	NOUN
eurjchem-2064	21	18	,	,	PUNCT
eurjchem-2064	21	19	and	and	CCONJ
eurjchem-2064	21	20	antidepressant	antidepressant	ADJ
eurjchem-2064	21	21	properties	property	NOUN
eurjchem-2064	21	22	,	,	PUNCT
eurjchem-2064	21	23	among	among	ADP
eurjchem-2064	21	24	others	other	NOUN
eurjchem-2064	21	25	[	[	X
eurjchem-2064	21	26	5	5	NUM
eurjchem-2064	21	27	-	-	SYM
eurjchem-2064	21	28	9	9	NUM
eurjchem-2064	21	29	]	]	PUNCT
eurjchem-2064	21	30	.	.	PUNCT
eurjchem-2064	22	1	improved	improve	VERB
eurjchem-2064	22	2	synthetic	synthetic	ADJ
eurjchem-2064	22	3	techniques	technique	NOUN
eurjchem-2064	22	4	are	be	AUX
eurjchem-2064	22	5	necessary	necessary	ADJ
eurjchem-2064	22	6	to	to	PART
eurjchem-2064	22	7	create	create	VERB
eurjchem-2064	22	8	novel	novel	ADJ
eurjchem-2064	22	9	sulfonamide	sulfonamide	NOUN
eurjchem-2064	22	10	structures	structure	NOUN
eurjchem-2064	22	11	and	and	CCONJ
eurjchem-2064	22	12	advance	advance	NOUN
eurjchem-2064	22	13	drug	drug	NOUN
eurjchem-2064	22	14	discovery	discovery	NOUN
eurjchem-2064	22	15	.	.	PUNCT
eurjchem-2064	23	1	a	a	DET
eurjchem-2064	23	2	review	review	NOUN
eurjchem-2064	23	3	of	of	ADP
eurjchem-2064	23	4	the	the	DET
eurjchem-2064	23	5	literature	literature	NOUN
eurjchem-2064	23	6	suggests	suggest	VERB
eurjchem-2064	23	7	the	the	DET
eurjchem-2064	23	8	amination	amination	NOUN
eurjchem-2064	23	9	of	of	ADP
eurjchem-2064	23	10	either	either	PRON
eurjchem-2064	23	11	sulfonyl	sulfonyl	NOUN
eurjchem-2064	23	12	halides	halide	NOUN
eurjchem-2064	23	13	or	or	CCONJ
eurjchem-2064	23	14	activated	activate	VERB
eurjchem-2064	23	15	sulfonic	sulfonic	ADJ
eurjchem-2064	23	16	acids	acid	NOUN
eurjchem-2064	23	17	as	as	ADP
eurjchem-2064	23	18	a	a	DET
eurjchem-2064	23	19	means	means	NOUN
eurjchem-2064	23	20	of	of	ADP
eurjchem-2064	23	21	effectively	effectively	ADV
eurjchem-2064	23	22	producing	produce	VERB
eurjchem-2064	23	23	sulfonamides	sulfonamide	NOUN
eurjchem-2064	23	24	[	[	X
eurjchem-2064	23	25	10,11	10,11	NOUN
eurjchem-2064	23	26	]	]	PUNCT
eurjchem-2064	23	27	.	.	PUNCT
eurjchem-2064	24	1	a	a	DET
eurjchem-2064	24	2	general	general	ADJ
eurjchem-2064	24	3	reaction	reaction	NOUN
eurjchem-2064	24	4	showing	show	VERB
eurjchem-2064	24	5	sulfonamide	sulfonamide	ADJ
eurjchem-2064	24	6	formation	formation	NOUN
eurjchem-2064	24	7	via	via	ADP
eurjchem-2064	24	8	the	the	DET
eurjchem-2064	24	9	treatment	treatment	NOUN
eurjchem-2064	24	10	of	of	ADP
eurjchem-2064	24	11	a	a	DET
eurjchem-2064	24	12	sulfonyl	sulfonyl	ADJ
eurjchem-2064	24	13	chloride	chloride	NOUN
eurjchem-2064	24	14	with	with	ADP
eurjchem-2064	24	15	an	an	DET
eurjchem-2064	24	16	amine	amine	NOUN
eurjchem-2064	24	17	can	can	AUX
eurjchem-2064	24	18	be	be	AUX
eurjchem-2064	24	19	found	find	VERB
eurjchem-2064	24	20	in	in	ADP
eurjchem-2064	24	21	figure	figure	NOUN
eurjchem-2064	24	22	1	1	NUM
eurjchem-2064	24	23	.	.	PUNCT
eurjchem-2064	24	24	tosylation	tosylation	NOUN
eurjchem-2064	24	25	of	of	ADP
eurjchem-2064	24	26	an	an	DET
eurjchem-2064	24	27	amine	amine	NOUN
eurjchem-2064	24	28	has	have	AUX
eurjchem-2064	24	29	been	be	AUX
eurjchem-2064	24	30	thought	think	VERB
eurjchem-2064	24	31	to	to	PART
eurjchem-2064	24	32	follow	follow	VERB
eurjchem-2064	24	33	an	an	DET
eurjchem-2064	24	34	analogous	analogous	ADJ
eurjchem-2064	24	35	nucleophilic	nucleophilic	ADJ
eurjchem-2064	24	36	acyl	acyl	NOUN
eurjchem-2064	24	37	substitution	substitution	NOUN
eurjchem-2064	24	38	mechanism	mechanism	NOUN
eurjchem-2064	25	1	[	[	X
eurjchem-2064	25	2	12	12	NUM
eurjchem-2064	25	3	]	]	PUNCT
eurjchem-2064	25	4	.	.	PUNCT
eurjchem-2064	26	1	an	an	DET
eurjchem-2064	26	2	hcl	hcl	PROPN
eurjchem-2064	26	3	scavenger	scavenger	NOUN
eurjchem-2064	26	4	is	be	AUX
eurjchem-2064	26	5	necessary	necessary	ADJ
eurjchem-2064	26	6	to	to	PART
eurjchem-2064	26	7	establish	establish	VERB
eurjchem-2064	26	8	an	an	DET
eurjchem-2064	26	9	equilibrium	equilibrium	NOUN
eurjchem-2064	26	10	that	that	PRON
eurjchem-2064	26	11	favors	favor	VERB
eurjchem-2064	26	12	product	product	NOUN
eurjchem-2064	26	13	formation	formation	NOUN
eurjchem-2064	26	14	.	.	PUNCT
eurjchem-2064	27	1	s	s	PART
eurjchem-2064	27	2	cl	cl	NOUN
eurjchem-2064	27	3	o	o	NOUN
eurjchem-2064	27	4	or1	or1	NOUN
eurjchem-2064	27	5	n	n	PRON
eurjchem-2064	27	6	r3	r3	PROPN
eurjchem-2064	27	7	h	h	NOUN
eurjchem-2064	27	8	r2	r2	PROPN
eurjchem-2064	27	9	s	s	PART
eurjchem-2064	27	10	o	o	NOUN
eurjchem-2064	27	11	or1	or1	PROPN
eurjchem-2064	27	12	n	n	PROPN
eurjchem-2064	27	13	r3	r3	PROPN
eurjchem-2064	27	14	r2	r2	PROPN
eurjchem-2064	27	15	electrophilic	electrophilic	PROPN
eurjchem-2064	27	16	partner	partner	NOUN
eurjchem-2064	27	17	nucleophilic	nucleophilic	PROPN
eurjchem-2064	27	18	partner	partner	NOUN
eurjchem-2064	27	19	sulfonamide	sulfonamide	NOUN
eurjchem-2064	27	20	product	product	NOUN
eurjchem-2064	27	21	base	base	NOUN
eurjchem-2064	27	22	figure	figure	NOUN
eurjchem-2064	27	23	1	1	NUM
eurjchem-2064	27	24	.	.	PUNCT
eurjchem-2064	28	1	general	general	ADJ
eurjchem-2064	28	2	reaction	reaction	NOUN
eurjchem-2064	28	3	for	for	ADP
eurjchem-2064	28	4	the	the	DET
eurjchem-2064	28	5	formation	formation	NOUN
eurjchem-2064	28	6	of	of	ADP
eurjchem-2064	28	7	sulfonamides	sulfonamide	NOUN
eurjchem-2064	28	8	from	from	ADP
eurjchem-2064	28	9	sulfonyl	sulfonyl	NOUN
eurjchem-2064	28	10	chloride	chloride	NOUN
eurjchem-2064	28	11	and	and	CCONJ
eurjchem-2064	28	12	an	an	DET
eurjchem-2064	28	13	amine	amine	NOUN
eurjchem-2064	28	14	.	.	PUNCT
eurjchem-2064	29	1	proper	proper	ADJ
eurjchem-2064	29	2	characterization	characterization	NOUN
eurjchem-2064	29	3	of	of	ADP
eurjchem-2064	29	4	novel	novel	ADJ
eurjchem-2064	29	5	sulfonamide	sulfonamide	NOUN
eurjchem-2064	29	6	structures	structure	NOUN
eurjchem-2064	29	7	gives	give	VERB
eurjchem-2064	29	8	insight	insight	NOUN
eurjchem-2064	29	9	into	into	ADP
eurjchem-2064	29	10	their	their	PRON
eurjchem-2064	29	11	biological	biological	ADJ
eurjchem-2064	29	12	applications	application	NOUN
eurjchem-2064	29	13	.	.	PUNCT
eurjchem-2064	30	1	reports	report	NOUN
eurjchem-2064	30	2	show	show	VERB
eurjchem-2064	30	3	that	that	SCONJ
eurjchem-2064	30	4	conformational	conformational	ADJ
eurjchem-2064	30	5	effects	effect	NOUN
eurjchem-2064	30	6	play	play	VERB
eurjchem-2064	30	7	an	an	DET
eurjchem-2064	30	8	essential	essential	ADJ
eurjchem-2064	30	9	role	role	NOUN
eurjchem-2064	30	10	in	in	ADP
eurjchem-2064	30	11	the	the	DET
eurjchem-2064	30	12	biological	biological	ADJ
eurjchem-2064	30	13	activity	activity	NOUN
eurjchem-2064	30	14	of	of	ADP
eurjchem-2064	30	15	sulfonamides	sulfonamide	NOUN
eurjchem-2064	30	16	[	[	X
eurjchem-2064	30	17	13,14	13,14	NUM
eurjchem-2064	30	18	]	]	PUNCT
eurjchem-2064	30	19	.	.	PUNCT
eurjchem-2064	31	1	obtaining	obtain	VERB
eurjchem-2064	31	2	a	a	DET
eurjchem-2064	31	3	reliable	reliable	ADJ
eurjchem-2064	31	4	structure	structure	NOUN
eurjchem-2064	31	5	for	for	ADP
eurjchem-2064	31	6	interpretation	interpretation	NOUN
eurjchem-2064	31	7	can	can	AUX
eurjchem-2064	31	8	be	be	AUX
eurjchem-2064	31	9	done	do	VERB
eurjchem-2064	31	10	by	by	ADP
eurjchem-2064	31	11	x	x	ADJ
eurjchem-2064	31	12	-	-	NOUN
eurjchem-2064	31	13	ray	ray	NOUN
eurjchem-2064	31	14	diffraction	diffraction	NOUN
eurjchem-2064	31	15	.	.	PUNCT
eurjchem-2064	32	1	the	the	DET
eurjchem-2064	32	2	information	information	NOUN
eurjchem-2064	32	3	revealed	reveal	VERB
eurjchem-2064	32	4	upon	upon	SCONJ
eurjchem-2064	32	5	characterization	characterization	NOUN
eurjchem-2064	32	6	is	be	AUX
eurjchem-2064	32	7	necessary	necessary	ADJ
eurjchem-2064	32	8	for	for	ADP
eurjchem-2064	32	9	determining	determine	VERB
eurjchem-2064	32	10	the	the	DET
eurjchem-2064	32	11	conformational	conformational	ADJ
eurjchem-2064	32	12	preferences	preference	NOUN
eurjchem-2064	32	13	and	and	CCONJ
eurjchem-2064	32	14	structureproperty	structureproperty	NOUN
eurjchem-2064	32	15	relationships	relationship	NOUN
eurjchem-2064	32	16	of	of	ADP
eurjchem-2064	32	17	sulfonamide	sulfonamide	ADJ
eurjchem-2064	32	18	derivatives	derivative	NOUN
eurjchem-2064	32	19	.	.	PUNCT
eurjchem-2064	33	1	with	with	ADP
eurjchem-2064	33	2	the	the	DET
eurjchem-2064	33	3	ongoing	ongoing	ADJ
eurjchem-2064	33	4	discovery	discovery	NOUN
eurjchem-2064	33	5	of	of	ADP
eurjchem-2064	33	6	sulfa	sulfa	NOUN
eurjchem-2064	33	7	drugs	drug	NOUN
eurjchem-2064	33	8	,	,	PUNCT
eurjchem-2064	33	9	optimizing	optimize	VERB
eurjchem-2064	33	10	methodology	methodology	NOUN
eurjchem-2064	33	11	for	for	ADP
eurjchem-2064	33	12	the	the	DET
eurjchem-2064	33	13	synthesis	synthesis	NOUN
eurjchem-2064	33	14	of	of	ADP
eurjchem-2064	33	15	sulfonamides	sulfonamide	NOUN
eurjchem-2064	33	16	becomes	become	VERB
eurjchem-2064	33	17	increasingly	increasingly	ADV
eurjchem-2064	33	18	essential	essential	ADJ
eurjchem-2064	33	19	.	.	PUNCT
eurjchem-2064	34	1	abstract	abstract	ADJ
eurjchem-2064	34	2	research	research	NOUN
eurjchem-2064	34	3	article	article	NOUN
eurjchem-2064	34	4	keywords	keyword	VERB
eurjchem-2064	34	5	https://dx.doi.org/10.5155/eurjchem.12.2.109-116.2064	https://dx.doi.org/10.5155/eurjchem.12.2.109-116.2064	PROPN
eurjchem-2064	34	6	https://www.eurjchem.com/	https://www.eurjchem.com/	PROPN
eurjchem-2064	34	7	https://dx.doi.org/10.5155/eurjchem.12.2.109-116.2064	https://dx.doi.org/10.5155/eurjchem.12.2.109-116.2064	PROPN
eurjchem-2064	34	8	mailto:stenforb@mail.gvsu.edu	mailto:stenforb@mail.gvsu.edu	PROPN
eurjchem-2064	34	9	mailto:ngassaf@gvsu.edu	mailto:ngassaf@gvsu.edu	PROPN
eurjchem-2064	34	10	mailto:ngassaf@gvsu.edu	mailto:ngassaf@gvsu.edu	PROPN
eurjchem-2064	34	11	http://www.eurjchem.com/	http://www.eurjchem.com/	NOUN
eurjchem-2064	34	12	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.12.2.109-116.2064&domain=pdf&date_stamp=2021-06-30	https://crossmark.crossref.org/dialog/?doi=10.5155/eurjchem.12.2.109-116.2064&domain=pdf&date_stamp=2021-06-30	NOUN
eurjchem-2064	34	13	110	110	NUM
eurjchem-2064	34	14	stenfors	stenfor	NOUN
eurjchem-2064	34	15	and	and	CCONJ
eurjchem-2064	34	16	ngassa	ngassa	NOUN
eurjchem-2064	34	17	/	/	SYM
eurjchem-2064	34	18	european	european	ADJ
eurjchem-2064	34	19	journal	journal	PROPN
eurjchem-2064	34	20	of	of	ADP
eurjchem-2064	34	21	chemistry	chemistry	NOUN
eurjchem-2064	34	22	12	12	NUM
eurjchem-2064	34	23	(	(	PUNCT
eurjchem-2064	34	24	2	2	NUM
eurjchem-2064	34	25	)	)	PUNCT
eurjchem-2064	34	26	(	(	PUNCT
eurjchem-2064	34	27	2021	2021	NUM
eurjchem-2064	34	28	)	)	PUNCT
eurjchem-2064	34	29	109	109	NUM
eurjchem-2064	34	30	-	-	SYM
eurjchem-2064	34	31	116	116	NUM
eurjchem-2064	34	32	2021	2021	NUM
eurjchem-2064	34	33	–	–	PUNCT
eurjchem-2064	34	34	european	european	ADJ
eurjchem-2064	34	35	journal	journal	NOUN
eurjchem-2064	34	36	of	of	ADP
eurjchem-2064	34	37	chemistry	chemistry	NOUN
eurjchem-2064	34	38	–	–	PUNCT
eurjchem-2064	34	39	cc	cc	NOUN
eurjchem-2064	34	40	by	by	ADP
eurjchem-2064	34	41	nc	nc	PROPN
eurjchem-2064	34	42	–	–	PUNCT
eurjchem-2064	34	43	doi	doi	NOUN
eurjchem-2064	34	44	:	:	PUNCT
eurjchem-2064	34	45	10.5155	10.5155	NUM
eurjchem-2064	34	46	/	/	SYM
eurjchem-2064	34	47	eurjchem.12.2.109	eurjchem.12.2.109	PROPN
eurjchem-2064	34	48	-	-	PUNCT
eurjchem-2064	34	49	116.2064	116.2064	NUM
eurjchem-2064	34	50	an	an	DET
eurjchem-2064	34	51	effective	effective	ADJ
eurjchem-2064	34	52	recrystallization	recrystallization	NOUN
eurjchem-2064	34	53	method	method	NOUN
eurjchem-2064	34	54	must	must	AUX
eurjchem-2064	34	55	be	be	AUX
eurjchem-2064	34	56	implemented	implement	VERB
eurjchem-2064	34	57	to	to	PART
eurjchem-2064	34	58	produce	produce	VERB
eurjchem-2064	34	59	products	product	NOUN
eurjchem-2064	34	60	of	of	ADP
eurjchem-2064	34	61	high	high	ADJ
eurjchem-2064	34	62	purity	purity	NOUN
eurjchem-2064	34	63	fit	fit	NOUN
eurjchem-2064	34	64	for	for	ADP
eurjchem-2064	34	65	x	x	NOUN
eurjchem-2064	34	66	-	-	NOUN
eurjchem-2064	34	67	ray	ray	NOUN
eurjchem-2064	34	68	diffraction	diffraction	NOUN
eurjchem-2064	34	69	.	.	PUNCT
eurjchem-2064	35	1	herein	herein	NOUN
eurjchem-2064	35	2	,	,	PUNCT
eurjchem-2064	35	3	we	we	PRON
eurjchem-2064	35	4	report	report	VERB
eurjchem-2064	35	5	improved	improved	ADJ
eurjchem-2064	35	6	methodology	methodology	NOUN
eurjchem-2064	35	7	towards	towards	ADP
eurjchem-2064	35	8	the	the	DET
eurjchem-2064	35	9	synthesis	synthesis	NOUN
eurjchem-2064	35	10	of	of	ADP
eurjchem-2064	35	11	4	4	NUM
eurjchem-2064	35	12	-	-	PUNCT
eurjchem-2064	35	13	methylbenzenesulfonamide	methylbenzenesulfonamide	NOUN
eurjchem-2064	35	14	derivatives	derivative	NOUN
eurjchem-2064	35	15	and	and	CCONJ
eurjchem-2064	35	16	characterization	characterization	NOUN
eurjchem-2064	35	17	of	of	ADP
eurjchem-2064	35	18	the	the	DET
eurjchem-2064	35	19	resulting	result	VERB
eurjchem-2064	35	20	crystal	crystal	NOUN
eurjchem-2064	35	21	structures	structure	NOUN
eurjchem-2064	35	22	.	.	PUNCT
eurjchem-2064	36	1	2	2	X
eurjchem-2064	36	2	.	.	X
eurjchem-2064	36	3	experimental	experimental	ADJ
eurjchem-2064	36	4	2.1	2.1	NUM
eurjchem-2064	36	5	.	.	PUNCT
eurjchem-2064	37	1	synthesis	synthesis	VERB
eurjchem-2064	37	2	the	the	DET
eurjchem-2064	37	3	reagents	reagent	NOUN
eurjchem-2064	37	4	used	use	VERB
eurjchem-2064	37	5	in	in	ADP
eurjchem-2064	37	6	the	the	DET
eurjchem-2064	37	7	synthesis	synthesis	NOUN
eurjchem-2064	37	8	of	of	ADP
eurjchem-2064	37	9	4	4	NUM
eurjchem-2064	37	10	-	-	PUNCT
eurjchem-2064	37	11	methylbenzene	methylbenzene	NOUN
eurjchem-2064	37	12	sulfonamides	sulfonamide	NOUN
eurjchem-2064	37	13	were	be	AUX
eurjchem-2064	37	14	obtained	obtain	VERB
eurjchem-2064	37	15	from	from	ADP
eurjchem-2064	37	16	commercial	commercial	ADJ
eurjchem-2064	37	17	sources	source	NOUN
eurjchem-2064	37	18	and	and	CCONJ
eurjchem-2064	37	19	used	use	VERB
eurjchem-2064	37	20	without	without	ADP
eurjchem-2064	37	21	further	further	ADJ
eurjchem-2064	37	22	purification	purification	NOUN
eurjchem-2064	37	23	.	.	PUNCT
eurjchem-2064	38	1	thin	thin	ADJ
eurjchem-2064	38	2	-	-	PUNCT
eurjchem-2064	38	3	layer	layer	NOUN
eurjchem-2064	38	4	chromatography	chromatography	NOUN
eurjchem-2064	38	5	(	(	PUNCT
eurjchem-2064	38	6	tlc	tlc	NOUN
eurjchem-2064	38	7	)	)	PUNCT
eurjchem-2064	38	8	was	be	AUX
eurjchem-2064	38	9	used	use	VERB
eurjchem-2064	38	10	to	to	PART
eurjchem-2064	38	11	track	track	VERB
eurjchem-2064	38	12	reaction	reaction	NOUN
eurjchem-2064	38	13	progress	progress	NOUN
eurjchem-2064	38	14	and	and	CCONJ
eurjchem-2064	38	15	obtain	obtain	VERB
eurjchem-2064	38	16	rf	rf	NUM
eurjchem-2064	38	17	values	value	NOUN
eurjchem-2064	38	18	for	for	ADP
eurjchem-2064	38	19	the	the	DET
eurjchem-2064	38	20	reactions	reaction	NOUN
eurjchem-2064	38	21	.	.	PUNCT
eurjchem-2064	39	1	results	result	NOUN
eurjchem-2064	39	2	were	be	AUX
eurjchem-2064	39	3	analyzed	analyze	VERB
eurjchem-2064	39	4	,	,	PUNCT
eurjchem-2064	39	5	and	and	CCONJ
eurjchem-2064	39	6	figures	figure	NOUN
eurjchem-2064	39	7	were	be	AUX
eurjchem-2064	39	8	created	create	VERB
eurjchem-2064	39	9	with	with	ADP
eurjchem-2064	39	10	the	the	DET
eurjchem-2064	39	11	use	use	NOUN
eurjchem-2064	39	12	of	of	ADP
eurjchem-2064	39	13	mestrenova	mestrenova	NOUN
eurjchem-2064	40	1	[	[	X
eurjchem-2064	40	2	15	15	NUM
eurjchem-2064	40	3	]	]	PUNCT
eurjchem-2064	40	4	.	.	PUNCT
eurjchem-2064	41	1	2.1.1	2.1.1	NUM
eurjchem-2064	41	2	.	.	PUNCT
eurjchem-2064	41	3	general	general	ADJ
eurjchem-2064	41	4	procedure	procedure	NOUN
eurjchem-2064	41	5	for	for	ADP
eurjchem-2064	41	6	the	the	DET
eurjchem-2064	41	7	preparation	preparation	NOUN
eurjchem-2064	41	8	of	of	ADP
eurjchem-2064	41	9	sulfonamides	sulfonamide	NOUN
eurjchem-2064	41	10	synthesized	synthesize	VERB
eurjchem-2064	41	11	in	in	ADP
eurjchem-2064	41	12	the	the	DET
eurjchem-2064	41	13	presence	presence	NOUN
eurjchem-2064	41	14	of	of	ADP
eurjchem-2064	41	15	pyridine	pyridine	NOUN
eurjchem-2064	41	16	(	(	PUNCT
eurjchem-2064	41	17	1	1	NUM
eurjchem-2064	41	18	-	-	SYM
eurjchem-2064	41	19	10	10	NUM
eurjchem-2064	41	20	)	)	PUNCT
eurjchem-2064	41	21	an	an	DET
eurjchem-2064	41	22	amine	amine	ADJ
eurjchem-2064	41	23	(	(	PUNCT
eurjchem-2064	41	24	5.90	5.90	NUM
eurjchem-2064	41	25	mmol	mmol	NOUN
eurjchem-2064	41	26	)	)	PUNCT
eurjchem-2064	41	27	was	be	AUX
eurjchem-2064	41	28	added	add	VERB
eurjchem-2064	41	29	to	to	ADP
eurjchem-2064	41	30	a	a	DET
eurjchem-2064	41	31	flask	flask	NOUN
eurjchem-2064	41	32	containing	contain	VERB
eurjchem-2064	41	33	10	10	NUM
eurjchem-2064	41	34	ml	ml	NOUN
eurjchem-2064	41	35	of	of	ADP
eurjchem-2064	41	36	ch2cl2	ch2cl2	NOUN
eurjchem-2064	41	37	.	.	PUNCT
eurjchem-2064	42	1	this	this	PRON
eurjchem-2064	42	2	was	be	AUX
eurjchem-2064	42	3	followed	follow	VERB
eurjchem-2064	42	4	by	by	ADP
eurjchem-2064	42	5	the	the	DET
eurjchem-2064	42	6	addition	addition	NOUN
eurjchem-2064	42	7	of	of	ADP
eurjchem-2064	42	8	pyridine	pyridine	NOUN
eurjchem-2064	42	9	(	(	PUNCT
eurjchem-2064	42	10	0.48	0.48	NUM
eurjchem-2064	42	11	ml	ml	NOUN
eurjchem-2064	42	12	,	,	PUNCT
eurjchem-2064	42	13	5.90	5.90	NUM
eurjchem-2064	42	14	mmol	mmol	NOUN
eurjchem-2064	42	15	)	)	PUNCT
eurjchem-2064	42	16	.	.	PUNCT
eurjchem-2064	43	1	the	the	DET
eurjchem-2064	43	2	solution	solution	NOUN
eurjchem-2064	43	3	was	be	AUX
eurjchem-2064	43	4	stirred	stir	VERB
eurjchem-2064	43	5	at	at	ADP
eurjchem-2064	43	6	room	room	NOUN
eurjchem-2064	43	7	temperate	temperate	NOUN
eurjchem-2064	43	8	for	for	ADP
eurjchem-2064	43	9	10	10	NUM
eurjchem-2064	43	10	minutes	minute	NOUN
eurjchem-2064	43	11	under	under	ADP
eurjchem-2064	43	12	n2	n2	ADJ
eurjchem-2064	43	13	atmosphere	atmosphere	NOUN
eurjchem-2064	43	14	.	.	PUNCT
eurjchem-2064	44	1	4	4	NUM
eurjchem-2064	44	2	-	-	PUNCT
eurjchem-2064	44	3	methyl	methyl	NOUN
eurjchem-2064	44	4	benzenesulfonyl	benzenesulfonyl	NOUN
eurjchem-2064	44	5	chloride	chloride	NOUN
eurjchem-2064	44	6	(	(	PUNCT
eurjchem-2064	44	7	1.00	1.00	NUM
eurjchem-2064	44	8	g	g	NOUN
eurjchem-2064	44	9	,	,	PUNCT
eurjchem-2064	44	10	5.25	5.25	NUM
eurjchem-2064	44	11	mmol	mmol	NOUN
eurjchem-2064	44	12	)	)	PUNCT
eurjchem-2064	44	13	was	be	AUX
eurjchem-2064	44	14	then	then	ADV
eurjchem-2064	44	15	added	add	VERB
eurjchem-2064	44	16	dropwise	dropwise	NOUN
eurjchem-2064	44	17	to	to	ADP
eurjchem-2064	44	18	the	the	DET
eurjchem-2064	44	19	solution	solution	NOUN
eurjchem-2064	44	20	.	.	PUNCT
eurjchem-2064	45	1	the	the	DET
eurjchem-2064	45	2	mixture	mixture	NOUN
eurjchem-2064	45	3	was	be	AUX
eurjchem-2064	45	4	stirred	stir	VERB
eurjchem-2064	45	5	at	at	ADP
eurjchem-2064	45	6	room	room	NOUN
eurjchem-2064	45	7	temperate	temperate	NOUN
eurjchem-2064	45	8	for	for	ADP
eurjchem-2064	45	9	24	24	NUM
eurjchem-2064	45	10	hours	hour	NOUN
eurjchem-2064	45	11	under	under	ADP
eurjchem-2064	45	12	n2	n2	ADJ
eurjchem-2064	45	13	atmosphere	atmosphere	NOUN
eurjchem-2064	45	14	.	.	PUNCT
eurjchem-2064	46	1	reaction	reaction	NOUN
eurjchem-2064	46	2	completion	completion	NOUN
eurjchem-2064	46	3	was	be	AUX
eurjchem-2064	46	4	verified	verify	VERB
eurjchem-2064	46	5	by	by	ADP
eurjchem-2064	46	6	tlc	tlc	NOUN
eurjchem-2064	46	7	analysis	analysis	NOUN
eurjchem-2064	46	8	.	.	PUNCT
eurjchem-2064	47	1	after	after	SCONJ
eurjchem-2064	47	2	the	the	DET
eurjchem-2064	47	3	mixture	mixture	NOUN
eurjchem-2064	47	4	was	be	AUX
eurjchem-2064	47	5	acidified	acidify	VERB
eurjchem-2064	47	6	with	with	ADP
eurjchem-2064	47	7	5	5	NUM
eurjchem-2064	47	8	m	m	NOUN
eurjchem-2064	47	9	hcl	hcl	NOUN
eurjchem-2064	47	10	and	and	CCONJ
eurjchem-2064	47	11	diluted	dilute	VERB
eurjchem-2064	47	12	with	with	ADP
eurjchem-2064	47	13	ch2cl2	ch2cl2	PROPN
eurjchem-2064	47	14	,	,	PUNCT
eurjchem-2064	47	15	the	the	DET
eurjchem-2064	47	16	organic	organic	ADJ
eurjchem-2064	47	17	layer	layer	NOUN
eurjchem-2064	47	18	was	be	AUX
eurjchem-2064	47	19	washed	wash	VERB
eurjchem-2064	47	20	three	three	NUM
eurjchem-2064	47	21	times	time	NOUN
eurjchem-2064	47	22	with	with	ADP
eurjchem-2064	47	23	h2o	h2o	PROPN
eurjchem-2064	47	24	.	.	PUNCT
eurjchem-2064	48	1	the	the	DET
eurjchem-2064	48	2	aqueous	aqueous	ADJ
eurjchem-2064	48	3	layer	layer	NOUN
eurjchem-2064	48	4	was	be	AUX
eurjchem-2064	48	5	back	back	ADV
eurjchem-2064	48	6	extracted	extract	VERB
eurjchem-2064	48	7	with	with	ADP
eurjchem-2064	48	8	ch2cl2	ch2cl2	NOUN
eurjchem-2064	48	9	,	,	PUNCT
eurjchem-2064	48	10	and	and	CCONJ
eurjchem-2064	48	11	the	the	DET
eurjchem-2064	48	12	organic	organic	ADJ
eurjchem-2064	48	13	layers	layer	NOUN
eurjchem-2064	48	14	were	be	AUX
eurjchem-2064	48	15	combined	combine	VERB
eurjchem-2064	48	16	and	and	CCONJ
eurjchem-2064	48	17	dried	dry	VERB
eurjchem-2064	48	18	over	over	ADP
eurjchem-2064	48	19	anhydrous	anhydrous	ADJ
eurjchem-2064	48	20	na2so4	na2so4	NOUN
eurjchem-2064	48	21	.	.	PUNCT
eurjchem-2064	49	1	after	after	ADP
eurjchem-2064	49	2	solvent	solvent	ADJ
eurjchem-2064	49	3	evaporation	evaporation	NOUN
eurjchem-2064	49	4	,	,	PUNCT
eurjchem-2064	49	5	the	the	DET
eurjchem-2064	49	6	residue	residue	NOUN
eurjchem-2064	49	7	was	be	AUX
eurjchem-2064	49	8	purified	purify	VERB
eurjchem-2064	49	9	using	use	VERB
eurjchem-2064	49	10	either	either	CCONJ
eurjchem-2064	49	11	recrystallization	recrystallization	NOUN
eurjchem-2064	49	12	in	in	ADP
eurjchem-2064	49	13	ethanol	ethanol	NOUN
eurjchem-2064	49	14	,	,	PUNCT
eurjchem-2064	49	15	or	or	CCONJ
eurjchem-2064	49	16	trituration	trituration	NOUN
eurjchem-2064	49	17	with	with	ADP
eurjchem-2064	49	18	petroleum	petroleum	NOUN
eurjchem-2064	49	19	ether	ether	NOUN
eurjchem-2064	49	20	or	or	CCONJ
eurjchem-2064	49	21	diethyl	diethyl	NOUN
eurjchem-2064	49	22	ether	ether	NOUN
eurjchem-2064	49	23	.	.	PUNCT
eurjchem-2064	50	1	the	the	DET
eurjchem-2064	50	2	recrystallized	recrystallize	VERB
eurjchem-2064	50	3	product	product	NOUN
eurjchem-2064	50	4	was	be	AUX
eurjchem-2064	50	5	isolated	isolate	VERB
eurjchem-2064	50	6	via	via	ADP
eurjchem-2064	50	7	vacuum	vacuum	NOUN
eurjchem-2064	50	8	filtration	filtration	NOUN
eurjchem-2064	50	9	to	to	PART
eurjchem-2064	50	10	afford	afford	VERB
eurjchem-2064	50	11	the	the	DET
eurjchem-2064	50	12	product	product	NOUN
eurjchem-2064	50	13	in	in	ADP
eurjchem-2064	50	14	good	good	ADJ
eurjchem-2064	50	15	purity	purity	NOUN
eurjchem-2064	50	16	and	and	CCONJ
eurjchem-2064	50	17	yield	yield	NOUN
eurjchem-2064	50	18	.	.	PUNCT
eurjchem-2064	51	1	n	n	CCONJ
eurjchem-2064	51	2	-	-	PUNCT
eurjchem-2064	51	3	benzyl	benzyl	NOUN
eurjchem-2064	51	4	-	-	PUNCT
eurjchem-2064	51	5	n,4	n,4	PRON
eurjchem-2064	51	6	-	-	PUNCT
eurjchem-2064	51	7	dimethylbenzenesulfonamide	dimethylbenzenesulfonamide	NOUN
eurjchem-2064	51	8	(	(	PUNCT
eurjchem-2064	51	9	1	1	NUM
eurjchem-2064	51	10	):	):	PUNCT
eurjchem-2064	51	11	transparent	transparent	ADJ
eurjchem-2064	51	12	crystals	crystal	NOUN
eurjchem-2064	51	13	.	.	PUNCT
eurjchem-2064	52	1	m.p	m.p	PROPN
eurjchem-2064	52	2	.	.	PROPN
eurjchem-2064	52	3	:	:	PUNCT
eurjchem-2064	53	1	101	101	NUM
eurjchem-2064	53	2	-	-	SYM
eurjchem-2064	53	3	103	103	NUM
eurjchem-2064	53	4	°	°	PROPN
eurjchem-2064	53	5	c	c	NOUN
eurjchem-2064	53	6	.	.	PUNCT
eurjchem-2064	54	1	rf	rf	VERB
eurjchem-2064	54	2	=	=	NOUN
eurjchem-2064	54	3	0.64	0.64	NUM
eurjchem-2064	54	4	(	(	PUNCT
eurjchem-2064	54	5	ch2cl2	ch2cl2	NOUN
eurjchem-2064	54	6	)	)	PUNCT
eurjchem-2064	54	7	.	.	PUNCT
eurjchem-2064	55	1	1h	1h	NUM
eurjchem-2064	55	2	nmr	nmr	NOUN
eurjchem-2064	55	3	(	(	PUNCT
eurjchem-2064	55	4	400	400	NUM
eurjchem-2064	55	5	mhz	mhz	NOUN
eurjchem-2064	55	6	,	,	PUNCT
eurjchem-2064	55	7	chloroform	chloroform	NOUN
eurjchem-2064	55	8	-	-	PUNCT
eurjchem-2064	55	9	d	d	PROPN
eurjchem-2064	55	10	,	,	PUNCT
eurjchem-2064	55	11	δ	δ	PROPN
eurjchem-2064	55	12	,	,	PUNCT
eurjchem-2064	55	13	ppm	ppm	NOUN
eurjchem-2064	55	14	):	):	PUNCT
eurjchem-2064	55	15	7.72	7.72	NUM
eurjchem-2064	55	16	(	(	PUNCT
eurjchem-2064	55	17	d	d	PROPN
eurjchem-2064	55	18	,	,	PUNCT
eurjchem-2064	55	19	j	j	PROPN
eurjchem-2064	55	20	=	=	PROPN
eurjchem-2064	55	21	8.2	8.2	NUM
eurjchem-2064	55	22	hz	hz	NOUN
eurjchem-2064	55	23	,	,	PUNCT
eurjchem-2064	55	24	2h	2h	NUM
eurjchem-2064	55	25	)	)	PUNCT
eurjchem-2064	55	26	,	,	PUNCT
eurjchem-2064	55	27	7.38	7.38	NUM
eurjchem-2064	55	28	-	-	SYM
eurjchem-2064	55	29	7.22	7.22	NUM
eurjchem-2064	55	30	(	(	PUNCT
eurjchem-2064	55	31	m	m	PROPN
eurjchem-2064	55	32	,	,	PUNCT
eurjchem-2064	55	33	7h	7h	PROPN
eurjchem-2064	55	34	)	)	PUNCT
eurjchem-2064	55	35	,	,	PUNCT
eurjchem-2064	55	36	4.11	4.11	NUM
eurjchem-2064	55	37	(	(	PUNCT
eurjchem-2064	55	38	s	s	PROPN
eurjchem-2064	55	39	,	,	PUNCT
eurjchem-2064	55	40	2h	2h	NUM
eurjchem-2064	55	41	)	)	PUNCT
eurjchem-2064	55	42	,	,	PUNCT
eurjchem-2064	55	43	2.57	2.57	NUM
eurjchem-2064	55	44	(	(	PUNCT
eurjchem-2064	55	45	s	s	PROPN
eurjchem-2064	55	46	,	,	PUNCT
eurjchem-2064	55	47	3h	3h	NUM
eurjchem-2064	55	48	)	)	PUNCT
eurjchem-2064	55	49	,	,	PUNCT
eurjchem-2064	55	50	2.45	2.45	NUM
eurjchem-2064	55	51	(	(	PUNCT
eurjchem-2064	55	52	s	s	PROPN
eurjchem-2064	55	53	,	,	PUNCT
eurjchem-2064	55	54	3h	3h	NUM
eurjchem-2064	55	55	)	)	PUNCT
eurjchem-2064	55	56	.	.	PUNCT
eurjchem-2064	56	1	13c	13c	NOUN
eurjchem-2064	56	2	nmr	nmr	NOUN
eurjchem-2064	56	3	(	(	PUNCT
eurjchem-2064	56	4	100	100	NUM
eurjchem-2064	56	5	mhz	mhz	NOUN
eurjchem-2064	56	6	,	,	PUNCT
eurjchem-2064	56	7	chloroform	chloroform	NOUN
eurjchem-2064	56	8	-	-	PUNCT
eurjchem-2064	56	9	d	d	PROPN
eurjchem-2064	56	10	,	,	PUNCT
eurjchem-2064	56	11	δ	δ	PROPN
eurjchem-2064	56	12	,	,	PUNCT
eurjchem-2064	56	13	ppm	ppm	NUM
eurjchem-2064	56	14	):	):	PUNCT
eurjchem-2064	56	15	143.59	143.59	NUM
eurjchem-2064	56	16	,	,	PUNCT
eurjchem-2064	56	17	135.78	135.78	NUM
eurjchem-2064	56	18	,	,	PUNCT
eurjchem-2064	56	19	134.33	134.33	NUM
eurjchem-2064	56	20	,	,	PUNCT
eurjchem-2064	56	21	129.87	129.87	NUM
eurjchem-2064	56	22	,	,	PUNCT
eurjchem-2064	56	23	128.74	128.74	NUM
eurjchem-2064	56	24	,	,	PUNCT
eurjchem-2064	56	25	128.49	128.49	NUM
eurjchem-2064	56	26	,	,	PUNCT
eurjchem-2064	56	27	127.99	127.99	NUM
eurjchem-2064	56	28	,	,	PUNCT
eurjchem-2064	56	29	127.64	127.64	NUM
eurjchem-2064	56	30	,	,	PUNCT
eurjchem-2064	56	31	54.24	54.24	NUM
eurjchem-2064	56	32	,	,	PUNCT
eurjchem-2064	56	33	34.44	34.44	NUM
eurjchem-2064	56	34	,	,	PUNCT
eurjchem-2064	56	35	21.66	21.66	NUM
eurjchem-2064	56	36	.	.	NOUN
eurjchem-2064	56	37	4	4	NUM
eurjchem-2064	56	38	-	-	PUNCT
eurjchem-2064	56	39	tosylmorpholine	tosylmorpholine	ADJ
eurjchem-2064	56	40	(	(	PUNCT
eurjchem-2064	56	41	2	2	NUM
eurjchem-2064	56	42	):	):	PUNCT
eurjchem-2064	56	43	transparent	transparent	ADJ
eurjchem-2064	56	44	,	,	PUNCT
eurjchem-2064	56	45	needle	needle	NOUN
eurjchem-2064	56	46	-	-	PUNCT
eurjchem-2064	56	47	like	like	ADJ
eurjchem-2064	56	48	crystals	crystal	NOUN
eurjchem-2064	56	49	.	.	PUNCT
eurjchem-2064	57	1	m.p	m.p	PROPN
eurjchem-2064	57	2	.	.	PROPN
eurjchem-2064	57	3	:	:	PUNCT
eurjchem-2064	58	1	157	157	NUM
eurjchem-2064	58	2	-	-	SYM
eurjchem-2064	58	3	160	160	NUM
eurjchem-2064	58	4	°	°	SYM
eurjchem-2064	58	5	c	c	NOUN
eurjchem-2064	58	6	.	.	PUNCT
eurjchem-2064	59	1	rf	rf	VERB
eurjchem-2064	59	2	=	=	NOUN
eurjchem-2064	59	3	0.31	0.31	NUM
eurjchem-2064	59	4	(	(	PUNCT
eurjchem-2064	59	5	ch2cl2	ch2cl2	NOUN
eurjchem-2064	59	6	)	)	PUNCT
eurjchem-2064	59	7	.	.	PUNCT
eurjchem-2064	60	1	1h	1h	NUM
eurjchem-2064	60	2	nmr	nmr	NOUN
eurjchem-2064	60	3	(	(	PUNCT
eurjchem-2064	60	4	400	400	NUM
eurjchem-2064	60	5	mhz	mhz	NOUN
eurjchem-2064	60	6	,	,	PUNCT
eurjchem-2064	60	7	chloroform	chloroform	NOUN
eurjchem-2064	60	8	-	-	PUNCT
eurjchem-2064	60	9	d	d	PROPN
eurjchem-2064	60	10	,	,	PUNCT
eurjchem-2064	60	11	δ	δ	PROPN
eurjchem-2064	60	12	,	,	PUNCT
eurjchem-2064	60	13	ppm	ppm	NUM
eurjchem-2064	60	14	):	):	PUNCT
eurjchem-2064	60	15	7.62	7.62	NUM
eurjchem-2064	60	16	(	(	PUNCT
eurjchem-2064	60	17	d	d	PROPN
eurjchem-2064	60	18	,	,	PUNCT
eurjchem-2064	60	19	j	j	PROPN
eurjchem-2064	60	20	=	=	SYM
eurjchem-2064	60	21	8.0	8.0	NUM
eurjchem-2064	60	22	hz	hz	NOUN
eurjchem-2064	60	23	,	,	PUNCT
eurjchem-2064	60	24	2h	2h	NUM
eurjchem-2064	60	25	)	)	PUNCT
eurjchem-2064	60	26	,	,	PUNCT
eurjchem-2064	60	27	7.33	7.33	NUM
eurjchem-2064	60	28	(	(	PUNCT
eurjchem-2064	60	29	d	d	PROPN
eurjchem-2064	60	30	,	,	PUNCT
eurjchem-2064	60	31	j	j	PROPN
eurjchem-2064	60	32	=	=	SYM
eurjchem-2064	60	33	7.9	7.9	NUM
eurjchem-2064	60	34	hz	hz	NOUN
eurjchem-2064	60	35	,	,	PUNCT
eurjchem-2064	60	36	2h	2h	NUM
eurjchem-2064	60	37	)	)	PUNCT
eurjchem-2064	60	38	,	,	PUNCT
eurjchem-2064	60	39	3.79	3.79	NUM
eurjchem-2064	60	40	-	-	SYM
eurjchem-2064	60	41	3.66	3.66	NUM
eurjchem-2064	60	42	(	(	PUNCT
eurjchem-2064	60	43	m	m	PROPN
eurjchem-2064	60	44	,	,	PUNCT
eurjchem-2064	60	45	4h	4h	NOUN
eurjchem-2064	60	46	)	)	PUNCT
eurjchem-2064	60	47	,	,	PUNCT
eurjchem-2064	60	48	2.96	2.96	NUM
eurjchem-2064	60	49	(	(	PUNCT
eurjchem-2064	60	50	t	t	PROPN
eurjchem-2064	60	51	,	,	PUNCT
eurjchem-2064	60	52	j	j	PROPN
eurjchem-2064	60	53	=	=	SYM
eurjchem-2064	60	54	4.8	4.8	NUM
eurjchem-2064	60	55	hz	hz	NOUN
eurjchem-2064	60	56	,	,	PUNCT
eurjchem-2064	60	57	4h	4h	NOUN
eurjchem-2064	60	58	)	)	PUNCT
eurjchem-2064	60	59	,	,	PUNCT
eurjchem-2064	60	60	2.43	2.43	NUM
eurjchem-2064	60	61	(	(	PUNCT
eurjchem-2064	60	62	s	s	PROPN
eurjchem-2064	60	63	,	,	PUNCT
eurjchem-2064	60	64	3h	3h	NUM
eurjchem-2064	60	65	)	)	PUNCT
eurjchem-2064	60	66	.	.	PUNCT
eurjchem-2064	61	1	13c	13c	NOUN
eurjchem-2064	61	2	nmr	nmr	NOUN
eurjchem-2064	61	3	(	(	PUNCT
eurjchem-2064	61	4	100	100	NUM
eurjchem-2064	61	5	mhz	mhz	NOUN
eurjchem-2064	61	6	,	,	PUNCT
eurjchem-2064	61	7	chloroform	chloroform	NOUN
eurjchem-2064	61	8	-	-	PUNCT
eurjchem-2064	61	9	d	d	PROPN
eurjchem-2064	61	10	,	,	PUNCT
eurjchem-2064	61	11	δ	δ	PROPN
eurjchem-2064	61	12	,	,	PUNCT
eurjchem-2064	61	13	ppm	ppm	NOUN
eurjchem-2064	61	14	):	):	PUNCT
eurjchem-2064	61	15	144.07	144.07	NUM
eurjchem-2064	61	16	,	,	PUNCT
eurjchem-2064	61	17	132.05	132.05	NUM
eurjchem-2064	61	18	,	,	PUNCT
eurjchem-2064	61	19	129.85	129.85	NUM
eurjchem-2064	61	20	,	,	PUNCT
eurjchem-2064	61	21	128.00	128.00	NUM
eurjchem-2064	61	22	,	,	PUNCT
eurjchem-2064	61	23	66.19	66.19	NUM
eurjchem-2064	61	24	,	,	PUNCT
eurjchem-2064	61	25	46.08	46.08	NUM
eurjchem-2064	61	26	,	,	PUNCT
eurjchem-2064	61	27	21.66	21.66	NUM
eurjchem-2064	61	28	.	.	NOUN
eurjchem-2064	61	29	1	1	NUM
eurjchem-2064	61	30	-	-	PUNCT
eurjchem-2064	61	31	tosylpyrrolidine	tosylpyrrolidine	NOUN
eurjchem-2064	61	32	(	(	PUNCT
eurjchem-2064	61	33	3	3	NUM
eurjchem-2064	61	34	):	):	PUNCT
eurjchem-2064	61	35	white	white	ADJ
eurjchem-2064	61	36	,	,	PUNCT
eurjchem-2064	61	37	needle	needle	NOUN
eurjchem-2064	61	38	-	-	PUNCT
eurjchem-2064	61	39	like	like	ADJ
eurjchem-2064	61	40	crystals	crystal	NOUN
eurjchem-2064	61	41	.	.	PUNCT
eurjchem-2064	62	1	m.p	m.p	PROPN
eurjchem-2064	62	2	.	.	PROPN
eurjchem-2064	62	3	:	:	PUNCT
eurjchem-2064	63	1	132	132	NUM
eurjchem-2064	63	2	-	-	SYM
eurjchem-2064	63	3	134	134	NUM
eurjchem-2064	63	4	°	°	NUM
eurjchem-2064	63	5	c	c	NOUN
eurjchem-2064	63	6	.	.	PUNCT
eurjchem-2064	64	1	rf	rf	NOUN
eurjchem-2064	64	2	=	=	NOUN
eurjchem-2064	64	3	0.35	0.35	NUM
eurjchem-2064	64	4	(	(	PUNCT
eurjchem-2064	64	5	ch2cl2	ch2cl2	NOUN
eurjchem-2064	64	6	)	)	PUNCT
eurjchem-2064	64	7	.	.	PUNCT
eurjchem-2064	65	1	1h	1h	NUM
eurjchem-2064	65	2	nmr	nmr	NOUN
eurjchem-2064	65	3	(	(	PUNCT
eurjchem-2064	65	4	400	400	NUM
eurjchem-2064	65	5	mhz	mhz	NOUN
eurjchem-2064	65	6	,	,	PUNCT
eurjchem-2064	65	7	chloroformd	chloroformd	PROPN
eurjchem-2064	65	8	,	,	PUNCT
eurjchem-2064	65	9	δ	δ	PROPN
eurjchem-2064	65	10	,	,	PUNCT
eurjchem-2064	65	11	ppm	ppm	NUM
eurjchem-2064	65	12	):	):	PUNCT
eurjchem-2064	65	13	7.74	7.74	NUM
eurjchem-2064	65	14	-	-	SYM
eurjchem-2064	65	15	7.67	7.67	NUM
eurjchem-2064	65	16	(	(	PUNCT
eurjchem-2064	65	17	m	m	PROPN
eurjchem-2064	65	18	,	,	PUNCT
eurjchem-2064	65	19	2h	2h	NUM
eurjchem-2064	65	20	)	)	PUNCT
eurjchem-2064	65	21	,	,	PUNCT
eurjchem-2064	65	22	7.30	7.30	NUM
eurjchem-2064	65	23	(	(	PUNCT
eurjchem-2064	65	24	d	d	PROPN
eurjchem-2064	65	25	,	,	PUNCT
eurjchem-2064	65	26	j	j	PROPN
eurjchem-2064	65	27	=	=	SYM
eurjchem-2064	65	28	8.0	8.0	NUM
eurjchem-2064	65	29	hz	hz	NOUN
eurjchem-2064	65	30	,	,	PUNCT
eurjchem-2064	65	31	2h	2h	NUM
eurjchem-2064	65	32	)	)	PUNCT
eurjchem-2064	65	33	,	,	PUNCT
eurjchem-2064	65	34	3.26	3.26	NUM
eurjchem-2064	65	35	-	-	SYM
eurjchem-2064	65	36	3.16	3.16	NUM
eurjchem-2064	65	37	(	(	PUNCT
eurjchem-2064	65	38	m	m	PROPN
eurjchem-2064	65	39	,	,	PUNCT
eurjchem-2064	65	40	4h	4h	NOUN
eurjchem-2064	65	41	)	)	PUNCT
eurjchem-2064	65	42	,	,	PUNCT
eurjchem-2064	65	43	2.42	2.42	NUM
eurjchem-2064	65	44	(	(	PUNCT
eurjchem-2064	65	45	s	s	PROPN
eurjchem-2064	65	46	,	,	PUNCT
eurjchem-2064	65	47	3h	3h	NUM
eurjchem-2064	65	48	)	)	PUNCT
eurjchem-2064	65	49	,	,	PUNCT
eurjchem-2064	65	50	1.79	1.79	NUM
eurjchem-2064	65	51	-	-	SYM
eurjchem-2064	65	52	1.67	1.67	NUM
eurjchem-2064	65	53	(	(	PUNCT
eurjchem-2064	65	54	m	m	PROPN
eurjchem-2064	65	55	,	,	PUNCT
eurjchem-2064	65	56	3h	3h	NUM
eurjchem-2064	65	57	)	)	PUNCT
eurjchem-2064	65	58	.	.	PUNCT
eurjchem-2064	66	1	13c	13c	NOUN
eurjchem-2064	66	2	nmr	nmr	NOUN
eurjchem-2064	66	3	(	(	PUNCT
eurjchem-2064	66	4	100	100	NUM
eurjchem-2064	66	5	mhz	mhz	NOUN
eurjchem-2064	66	6	,	,	PUNCT
eurjchem-2064	66	7	chloroform	chloroform	NOUN
eurjchem-2064	66	8	-	-	PUNCT
eurjchem-2064	66	9	d	d	PROPN
eurjchem-2064	66	10	,	,	PUNCT
eurjchem-2064	66	11	δ	δ	PROPN
eurjchem-2064	66	12	,	,	PUNCT
eurjchem-2064	66	13	ppm	ppm	NOUN
eurjchem-2064	66	14	):	):	PUNCT
eurjchem-2064	66	15	143.39	143.39	NUM
eurjchem-2064	66	16	,	,	PUNCT
eurjchem-2064	66	17	133.94	133.94	NUM
eurjchem-2064	66	18	,	,	PUNCT
eurjchem-2064	66	19	129.70	129.70	NUM
eurjchem-2064	66	20	,	,	PUNCT
eurjchem-2064	66	21	127.67	127.67	NUM
eurjchem-2064	66	22	,	,	PUNCT
eurjchem-2064	66	23	48.00	48.00	NUM
eurjchem-2064	66	24	,	,	PUNCT
eurjchem-2064	66	25	25.29	25.29	NUM
eurjchem-2064	66	26	,	,	PUNCT
eurjchem-2064	66	27	21.63	21.63	NUM
eurjchem-2064	66	28	.	.	PUNCT
eurjchem-2064	67	1	n	n	CCONJ
eurjchem-2064	67	2	-	-	PUNCT
eurjchem-2064	67	3	butyl-4	butyl-4	NOUN
eurjchem-2064	67	4	-	-	PUNCT
eurjchem-2064	67	5	methylbenzenesulfonamide	methylbenzenesulfonamide	NOUN
eurjchem-2064	67	6	(	(	PUNCT
eurjchem-2064	67	7	4	4	NUM
eurjchem-2064	67	8	):	):	PUNCT
eurjchem-2064	67	9	transparent	transparent	ADJ
eurjchem-2064	67	10	crystals	crystal	NOUN
eurjchem-2064	67	11	.	.	PUNCT
eurjchem-2064	68	1	m.p	m.p	PROPN
eurjchem-2064	68	2	.	.	PROPN
eurjchem-2064	68	3	:	:	PUNCT
eurjchem-2064	69	1	51	51	NUM
eurjchem-2064	69	2	-	-	SYM
eurjchem-2064	69	3	53	53	NUM
eurjchem-2064	69	4	°	°	PROPN
eurjchem-2064	69	5	c	c	NOUN
eurjchem-2064	69	6	.	.	PUNCT
eurjchem-2064	70	1	rf	rf	NOUN
eurjchem-2064	70	2	=	=	NOUN
eurjchem-2064	70	3	0.33	0.33	NUM
eurjchem-2064	70	4	(	(	PUNCT
eurjchem-2064	70	5	ch2cl2	ch2cl2	NOUN
eurjchem-2064	70	6	)	)	PUNCT
eurjchem-2064	70	7	.	.	PUNCT
eurjchem-2064	71	1	1h	1h	NUM
eurjchem-2064	71	2	nmr	nmr	NOUN
eurjchem-2064	71	3	(	(	PUNCT
eurjchem-2064	71	4	400	400	NUM
eurjchem-2064	71	5	mhz	mhz	NOUN
eurjchem-2064	71	6	,	,	PUNCT
eurjchem-2064	71	7	chloroform	chloroform	NOUN
eurjchem-2064	71	8	-	-	PUNCT
eurjchem-2064	71	9	d	d	PROPN
eurjchem-2064	71	10	,	,	PUNCT
eurjchem-2064	71	11	δ	δ	PROPN
eurjchem-2064	71	12	,	,	PUNCT
eurjchem-2064	71	13	ppm	ppm	NUM
eurjchem-2064	71	14	):	):	PUNCT
eurjchem-2064	71	15	7.74	7.74	NUM
eurjchem-2064	71	16	(	(	PUNCT
eurjchem-2064	71	17	d	d	PROPN
eurjchem-2064	71	18	,	,	PUNCT
eurjchem-2064	71	19	j	j	PROPN
eurjchem-2064	71	20	=	=	PROPN
eurjchem-2064	71	21	8.2	8.2	NUM
eurjchem-2064	71	22	hz	hz	NOUN
eurjchem-2064	71	23	,	,	PUNCT
eurjchem-2064	71	24	2h	2h	NUM
eurjchem-2064	71	25	)	)	PUNCT
eurjchem-2064	71	26	,	,	PUNCT
eurjchem-2064	71	27	7.33	7.33	NUM
eurjchem-2064	71	28	-	-	SYM
eurjchem-2064	71	29	7.23	7.23	NUM
eurjchem-2064	71	30	(	(	PUNCT
eurjchem-2064	71	31	m	m	PROPN
eurjchem-2064	71	32	,	,	PUNCT
eurjchem-2064	71	33	2h	2h	NUM
eurjchem-2064	71	34	)	)	PUNCT
eurjchem-2064	71	35	,	,	PUNCT
eurjchem-2064	71	36	4.46	4.46	NUM
eurjchem-2064	71	37	(	(	PUNCT
eurjchem-2064	71	38	d	d	NOUN
eurjchem-2064	71	39	,	,	PUNCT
eurjchem-2064	71	40	j	j	PROPN
eurjchem-2064	72	1	=	=	SYM
eurjchem-2064	72	2	8.4	8.4	NUM
eurjchem-2064	72	3	hz	hz	NOUN
eurjchem-2064	72	4	,	,	PUNCT
eurjchem-2064	72	5	1h	1h	NUM
eurjchem-2064	72	6	)	)	PUNCT
eurjchem-2064	72	7	,	,	PUNCT
eurjchem-2064	72	8	2.91	2.91	NUM
eurjchem-2064	72	9	(	(	PUNCT
eurjchem-2064	72	10	q	q	NOUN
eurjchem-2064	72	11	,	,	PUNCT
eurjchem-2064	72	12	j	j	PROPN
eurjchem-2064	73	1	=	=	SYM
eurjchem-2064	73	2	6.8	6.8	NUM
eurjchem-2064	73	3	hz	hz	NOUN
eurjchem-2064	73	4	,	,	PUNCT
eurjchem-2064	73	5	2h	2h	NUM
eurjchem-2064	73	6	)	)	PUNCT
eurjchem-2064	73	7	,	,	PUNCT
eurjchem-2064	73	8	2.41	2.41	NUM
eurjchem-2064	73	9	(	(	PUNCT
eurjchem-2064	73	10	s	s	PROPN
eurjchem-2064	73	11	,	,	PUNCT
eurjchem-2064	73	12	3h	3h	NUM
eurjchem-2064	73	13	)	)	PUNCT
eurjchem-2064	73	14	,	,	PUNCT
eurjchem-2064	73	15	1.42	1.42	NUM
eurjchem-2064	73	16	(	(	PUNCT
eurjchem-2064	73	17	qd	qd	PROPN
eurjchem-2064	73	18	,	,	PUNCT
eurjchem-2064	73	19	j	j	PROPN
eurjchem-2064	74	1	=	=	NOUN
eurjchem-2064	74	2	7.3	7.3	NUM
eurjchem-2064	74	3	,	,	PUNCT
eurjchem-2064	74	4	5.9	5.9	NUM
eurjchem-2064	74	5	hz	hz	NOUN
eurjchem-2064	74	6	,	,	PUNCT
eurjchem-2064	74	7	2h	2h	NUM
eurjchem-2064	74	8	)	)	PUNCT
eurjchem-2064	74	9	,	,	PUNCT
eurjchem-2064	74	10	1.28	1.28	NUM
eurjchem-2064	74	11	(	(	PUNCT
eurjchem-2064	74	12	dt	dt	PROPN
eurjchem-2064	74	13	,	,	PUNCT
eurjchem-2064	74	14	j	j	PROPN
eurjchem-2064	74	15	=	=	SYM
eurjchem-2064	74	16	14.8	14.8	NUM
eurjchem-2064	74	17	,	,	PUNCT
eurjchem-2064	74	18	7.3	7.3	NUM
eurjchem-2064	74	19	hz	hz	NOUN
eurjchem-2064	74	20	,	,	PUNCT
eurjchem-2064	74	21	2h	2h	NUM
eurjchem-2064	74	22	)	)	PUNCT
eurjchem-2064	74	23	,	,	PUNCT
eurjchem-2064	74	24	0.83	0.83	NUM
eurjchem-2064	74	25	(	(	PUNCT
eurjchem-2064	74	26	t	t	PROPN
eurjchem-2064	74	27	,	,	PUNCT
eurjchem-2064	74	28	j	j	PROPN
eurjchem-2064	75	1	=	=	SYM
eurjchem-2064	75	2	7.3	7.3	NUM
eurjchem-2064	75	3	hz	hz	NOUN
eurjchem-2064	75	4	,	,	PUNCT
eurjchem-2064	75	5	3h	3h	NUM
eurjchem-2064	75	6	)	)	PUNCT
eurjchem-2064	75	7	.	.	PUNCT
eurjchem-2064	76	1	13c	13c	NOUN
eurjchem-2064	76	2	nmr	nmr	NOUN
eurjchem-2064	76	3	(	(	PUNCT
eurjchem-2064	76	4	100	100	NUM
eurjchem-2064	76	5	mhz	mhz	NOUN
eurjchem-2064	76	6	,	,	PUNCT
eurjchem-2064	76	7	chloroform	chloroform	NOUN
eurjchem-2064	76	8	-	-	PUNCT
eurjchem-2064	76	9	d	d	PROPN
eurjchem-2064	76	10	,	,	PUNCT
eurjchem-2064	76	11	δ	δ	PROPN
eurjchem-2064	76	12	,	,	PUNCT
eurjchem-2064	76	13	ppm	ppm	NUM
eurjchem-2064	76	14	):	):	PUNCT
eurjchem-2064	76	15	143.44	143.44	NUM
eurjchem-2064	76	16	,	,	PUNCT
eurjchem-2064	76	17	137.01	137.01	NUM
eurjchem-2064	76	18	,	,	PUNCT
eurjchem-2064	76	19	129.79	129.79	NUM
eurjchem-2064	76	20	,	,	PUNCT
eurjchem-2064	76	21	127.20	127.20	NUM
eurjchem-2064	76	22	,	,	PUNCT
eurjchem-2064	76	23	43.02	43.02	NUM
eurjchem-2064	76	24	,	,	PUNCT
eurjchem-2064	76	25	31.66	31.66	NUM
eurjchem-2064	76	26	,	,	PUNCT
eurjchem-2064	76	27	21.63	21.63	NUM
eurjchem-2064	76	28	,	,	PUNCT
eurjchem-2064	76	29	19.78	19.78	NUM
eurjchem-2064	76	30	,	,	PUNCT
eurjchem-2064	76	31	13.63	13.63	NUM
eurjchem-2064	76	32	.	.	PUNCT
eurjchem-2064	77	1	1	1	NUM
eurjchem-2064	77	2	-	-	PUNCT
eurjchem-2064	77	3	tosylpiperidine	tosylpiperidine	NOUN
eurjchem-2064	77	4	(	(	PUNCT
eurjchem-2064	77	5	5	5	NUM
eurjchem-2064	77	6	):	):	PUNCT
eurjchem-2064	77	7	transparent	transparent	ADJ
eurjchem-2064	77	8	crystals	crystal	NOUN
eurjchem-2064	77	9	.	.	PUNCT
eurjchem-2064	78	1	m.p	m.p	PROPN
eurjchem-2064	78	2	.	.	PROPN
eurjchem-2064	78	3	:	:	PUNCT
eurjchem-2064	79	1	104	104	NUM
eurjchem-2064	79	2	-	-	SYM
eurjchem-2064	79	3	106	106	NUM
eurjchem-2064	79	4	°	°	SYM
eurjchem-2064	79	5	c	c	NOUN
eurjchem-2064	79	6	.	.	PUNCT
eurjchem-2064	80	1	rf	rf	VERB
eurjchem-2064	80	2	=	=	NOUN
eurjchem-2064	80	3	0.52	0.52	NUM
eurjchem-2064	80	4	(	(	PUNCT
eurjchem-2064	80	5	ch2cl2	ch2cl2	NOUN
eurjchem-2064	80	6	)	)	PUNCT
eurjchem-2064	80	7	.	.	PUNCT
eurjchem-2064	81	1	1h	1h	NUM
eurjchem-2064	81	2	nmr	nmr	NOUN
eurjchem-2064	81	3	(	(	PUNCT
eurjchem-2064	81	4	400	400	NUM
eurjchem-2064	81	5	mhz	mhz	NOUN
eurjchem-2064	81	6	,	,	PUNCT
eurjchem-2064	81	7	chloroform	chloroform	NOUN
eurjchem-2064	81	8	-	-	PUNCT
eurjchem-2064	81	9	d	d	PROPN
eurjchem-2064	81	10	,	,	PUNCT
eurjchem-2064	81	11	δ	δ	PROPN
eurjchem-2064	81	12	,	,	PUNCT
eurjchem-2064	81	13	ppm	ppm	NOUN
eurjchem-2064	81	14	):	):	PUNCT
eurjchem-2064	81	15	7.65	7.65	NUM
eurjchem-2064	81	16	-	-	SYM
eurjchem-2064	81	17	7.60	7.60	NUM
eurjchem-2064	81	18	(	(	PUNCT
eurjchem-2064	81	19	d	d	PROPN
eurjchem-2064	81	20	,	,	PUNCT
eurjchem-2064	81	21	2h	2h	NUM
eurjchem-2064	81	22	)	)	PUNCT
eurjchem-2064	81	23	,	,	PUNCT
eurjchem-2064	81	24	7.30	7.30	NUM
eurjchem-2064	81	25	(	(	PUNCT
eurjchem-2064	81	26	d	d	PROPN
eurjchem-2064	81	27	,	,	PUNCT
eurjchem-2064	81	28	j	j	PROPN
eurjchem-2064	81	29	=	=	SYM
eurjchem-2064	81	30	8.0	8.0	NUM
eurjchem-2064	81	31	hz	hz	NOUN
eurjchem-2064	81	32	,	,	PUNCT
eurjchem-2064	81	33	2h	2h	NUM
eurjchem-2064	81	34	)	)	PUNCT
eurjchem-2064	81	35	,	,	PUNCT
eurjchem-2064	81	36	3.00	3.00	NUM
eurjchem-2064	81	37	-	-	SYM
eurjchem-2064	81	38	2.89	2.89	NUM
eurjchem-2064	81	39	(	(	PUNCT
eurjchem-2064	81	40	m	m	PROPN
eurjchem-2064	81	41	,	,	PUNCT
eurjchem-2064	81	42	4h	4h	NOUN
eurjchem-2064	81	43	)	)	PUNCT
eurjchem-2064	81	44	,	,	PUNCT
eurjchem-2064	81	45	2.42	2.42	NUM
eurjchem-2064	81	46	(	(	PUNCT
eurjchem-2064	81	47	s	s	PROPN
eurjchem-2064	81	48	,	,	PUNCT
eurjchem-2064	81	49	3h	3h	NUM
eurjchem-2064	81	50	)	)	PUNCT
eurjchem-2064	81	51	,	,	PUNCT
eurjchem-2064	81	52	1.68	1.68	NUM
eurjchem-2064	81	53	-	-	SYM
eurjchem-2064	81	54	1.58	1.58	NUM
eurjchem-2064	81	55	(	(	PUNCT
eurjchem-2064	81	56	m	m	PROPN
eurjchem-2064	81	57	,	,	PUNCT
eurjchem-2064	81	58	4h	4h	NOUN
eurjchem-2064	81	59	)	)	PUNCT
eurjchem-2064	81	60	,	,	PUNCT
eurjchem-2064	81	61	1.44	1.44	NUM
eurjchem-2064	81	62	-	-	SYM
eurjchem-2064	81	63	1.35	1.35	NUM
eurjchem-2064	81	64	(	(	PUNCT
eurjchem-2064	81	65	m	m	PROPN
eurjchem-2064	81	66	,	,	PUNCT
eurjchem-2064	81	67	2h	2h	NUM
eurjchem-2064	81	68	)	)	PUNCT
eurjchem-2064	81	69	.	.	PUNCT
eurjchem-2064	82	1	13c	13c	NOUN
eurjchem-2064	82	2	nmr	nmr	NOUN
eurjchem-2064	82	3	(	(	PUNCT
eurjchem-2064	82	4	100	100	NUM
eurjchem-2064	82	5	mhz	mhz	NOUN
eurjchem-2064	82	6	,	,	PUNCT
eurjchem-2064	82	7	chloroform	chloroform	NOUN
eurjchem-2064	82	8	-	-	PUNCT
eurjchem-2064	82	9	d	d	PROPN
eurjchem-2064	82	10	,	,	PUNCT
eurjchem-2064	82	11	δ	δ	PROPN
eurjchem-2064	82	12	,	,	PUNCT
eurjchem-2064	82	13	ppm	ppm	NOUN
eurjchem-2064	82	14	):	):	PUNCT
eurjchem-2064	82	15	143.39	143.39	NUM
eurjchem-2064	82	16	,	,	PUNCT
eurjchem-2064	82	17	133.29	133.29	NUM
eurjchem-2064	82	18	,	,	PUNCT
eurjchem-2064	82	19	129.64	129.64	NUM
eurjchem-2064	82	20	,	,	PUNCT
eurjchem-2064	82	21	127.83	127.83	NUM
eurjchem-2064	82	22	,	,	PUNCT
eurjchem-2064	82	23	47.03	47.03	NUM
eurjchem-2064	82	24	,	,	PUNCT
eurjchem-2064	82	25	25.24	25.24	NUM
eurjchem-2064	82	26	,	,	PUNCT
eurjchem-2064	82	27	23.61	23.61	NUM
eurjchem-2064	82	28	,	,	PUNCT
eurjchem-2064	82	29	21.63	21.63	NUM
eurjchem-2064	82	30	.	.	PUNCT
eurjchem-2064	83	1	n	n	CCONJ
eurjchem-2064	83	2	,	,	PUNCT
eurjchem-2064	83	3	n	n	CCONJ
eurjchem-2064	83	4	-	-	PUNCT
eurjchem-2064	83	5	dibenzyl-4	dibenzyl-4	NOUN
eurjchem-2064	83	6	-	-	PUNCT
eurjchem-2064	83	7	methylbenzenesulfonamide	methylbenzenesulfonamide	NOUN
eurjchem-2064	83	8	(	(	PUNCT
eurjchem-2064	83	9	6	6	NUM
eurjchem-2064	83	10	):	):	PUNCT
eurjchem-2064	83	11	white	white	ADJ
eurjchem-2064	83	12	crystalline	crystalline	NOUN
eurjchem-2064	83	13	sheets	sheet	NOUN
eurjchem-2064	83	14	.	.	PUNCT
eurjchem-2064	84	1	m.p	m.p	PROPN
eurjchem-2064	84	2	.	.	PROPN
eurjchem-2064	84	3	:	:	PUNCT
eurjchem-2064	85	1	83	83	NUM
eurjchem-2064	85	2	-	-	SYM
eurjchem-2064	85	3	87	87	NUM
eurjchem-2064	85	4	°	°	SYM
eurjchem-2064	85	5	c	c	NOUN
eurjchem-2064	85	6	.	.	PUNCT
eurjchem-2064	86	1	rf	rf	NOUN
eurjchem-2064	86	2	=	=	NOUN
eurjchem-2064	86	3	0.62	0.62	NUM
eurjchem-2064	86	4	(	(	PUNCT
eurjchem-2064	86	5	ch2cl2	ch2cl2	NOUN
eurjchem-2064	86	6	)	)	PUNCT
eurjchem-2064	86	7	.	.	PUNCT
eurjchem-2064	87	1	1h	1h	NUM
eurjchem-2064	87	2	nmr	nmr	NOUN
eurjchem-2064	87	3	(	(	PUNCT
eurjchem-2064	87	4	400	400	NUM
eurjchem-2064	87	5	mhz	mhz	NOUN
eurjchem-2064	87	6	,	,	PUNCT
eurjchem-2064	87	7	chloroform	chloroform	NOUN
eurjchem-2064	87	8	-	-	PUNCT
eurjchem-2064	87	9	d	d	PROPN
eurjchem-2064	87	10	,	,	PUNCT
eurjchem-2064	87	11	δ	δ	PROPN
eurjchem-2064	87	12	,	,	PUNCT
eurjchem-2064	87	13	ppm	ppm	NOUN
eurjchem-2064	87	14	):	):	PUNCT
eurjchem-2064	87	15	7.72	7.72	NUM
eurjchem-2064	87	16	(	(	PUNCT
eurjchem-2064	87	17	d	d	PROPN
eurjchem-2064	87	18	,	,	PUNCT
eurjchem-2064	87	19	j	j	PROPN
eurjchem-2064	87	20	=	=	SYM
eurjchem-2064	87	21	8.1	8.1	NUM
eurjchem-2064	87	22	hz	hz	NOUN
eurjchem-2064	87	23	,	,	PUNCT
eurjchem-2064	87	24	2h	2h	NUM
eurjchem-2064	87	25	)	)	PUNCT
eurjchem-2064	87	26	,	,	PUNCT
eurjchem-2064	87	27	7.29	7.29	NUM
eurjchem-2064	87	28	(	(	PUNCT
eurjchem-2064	87	29	d	d	PROPN
eurjchem-2064	87	30	,	,	PUNCT
eurjchem-2064	87	31	j	j	PROPN
eurjchem-2064	88	1	=	=	SYM
eurjchem-2064	88	2	8.0	8.0	NUM
eurjchem-2064	88	3	hz	hz	NOUN
eurjchem-2064	88	4	,	,	PUNCT
eurjchem-2064	88	5	2h	2h	NUM
eurjchem-2064	88	6	)	)	PUNCT
eurjchem-2064	88	7	,	,	PUNCT
eurjchem-2064	88	8	7.23	7.23	NUM
eurjchem-2064	88	9	-	-	SYM
eurjchem-2064	88	10	7.16	7.16	NUM
eurjchem-2064	88	11	(	(	PUNCT
eurjchem-2064	88	12	m	m	PROPN
eurjchem-2064	88	13	,	,	PUNCT
eurjchem-2064	88	14	6h	6h	NUM
eurjchem-2064	88	15	)	)	PUNCT
eurjchem-2064	88	16	,	,	PUNCT
eurjchem-2064	88	17	7.07	7.07	NUM
eurjchem-2064	88	18	-	-	SYM
eurjchem-2064	88	19	6.99	6.99	NUM
eurjchem-2064	88	20	(	(	PUNCT
eurjchem-2064	88	21	m	m	PROPN
eurjchem-2064	88	22	,	,	PUNCT
eurjchem-2064	88	23	4h	4h	NOUN
eurjchem-2064	88	24	)	)	PUNCT
eurjchem-2064	88	25	,	,	PUNCT
eurjchem-2064	88	26	4.29	4.29	NUM
eurjchem-2064	88	27	(	(	PUNCT
eurjchem-2064	88	28	s	s	PROPN
eurjchem-2064	88	29	,	,	PUNCT
eurjchem-2064	88	30	4h	4h	NOUN
eurjchem-2064	88	31	)	)	PUNCT
eurjchem-2064	88	32	,	,	PUNCT
eurjchem-2064	88	33	2.43	2.43	NUM
eurjchem-2064	88	34	(	(	PUNCT
eurjchem-2064	88	35	s	s	PROPN
eurjchem-2064	88	36	,	,	PUNCT
eurjchem-2064	88	37	3h	3h	NUM
eurjchem-2064	88	38	)	)	PUNCT
eurjchem-2064	88	39	.	.	PUNCT
eurjchem-2064	89	1	13c	13c	NOUN
eurjchem-2064	89	2	nmr	nmr	NOUN
eurjchem-2064	89	3	(	(	PUNCT
eurjchem-2064	89	4	100	100	NUM
eurjchem-2064	89	5	mhz	mhz	NOUN
eurjchem-2064	89	6	,	,	PUNCT
eurjchem-2064	89	7	chloroform	chloroform	NOUN
eurjchem-2064	89	8	-	-	PUNCT
eurjchem-2064	89	9	d	d	PROPN
eurjchem-2064	89	10	,	,	PUNCT
eurjchem-2064	89	11	δ	δ	PROPN
eurjchem-2064	89	12	,	,	PUNCT
eurjchem-2064	89	13	ppm	ppm	NOUN
eurjchem-2064	89	14	):	):	PUNCT
eurjchem-2064	89	15	143.39	143.39	NUM
eurjchem-2064	89	16	,	,	PUNCT
eurjchem-2064	89	17	137.77	137.77	NUM
eurjchem-2064	89	18	,	,	PUNCT
eurjchem-2064	89	19	135.76	135.76	NUM
eurjchem-2064	89	20	,	,	PUNCT
eurjchem-2064	89	21	129.81	129.81	NUM
eurjchem-2064	89	22	,	,	PUNCT
eurjchem-2064	89	23	128.67	128.67	NUM
eurjchem-2064	89	24	,	,	PUNCT
eurjchem-2064	89	25	128.50	128.50	NUM
eurjchem-2064	89	26	,	,	PUNCT
eurjchem-2064	89	27	127.72	127.72	NUM
eurjchem-2064	89	28	,	,	PUNCT
eurjchem-2064	89	29	127.35	127.35	NUM
eurjchem-2064	89	30	,	,	PUNCT
eurjchem-2064	89	31	58.59	58.59	NUM
eurjchem-2064	89	32	,	,	PUNCT
eurjchem-2064	89	33	50.54	50.54	NUM
eurjchem-2064	89	34	,	,	PUNCT
eurjchem-2064	89	35	21.65	21.65	NUM
eurjchem-2064	89	36	,	,	PUNCT
eurjchem-2064	89	37	18.53	18.53	NUM
eurjchem-2064	89	38	.	.	PUNCT
eurjchem-2064	90	1	n	n	CCONJ
eurjchem-2064	90	2	-	-	PUNCT
eurjchem-2064	90	3	allyl-4	allyl-4	NOUN
eurjchem-2064	90	4	-	-	PUNCT
eurjchem-2064	90	5	methylbenzenesulfonamide	methylbenzenesulfonamide	NOUN
eurjchem-2064	90	6	(	(	PUNCT
eurjchem-2064	90	7	7	7	NUM
eurjchem-2064	90	8	):	):	PUNCT
eurjchem-2064	90	9	transparent	transparent	ADJ
eurjchem-2064	90	10	crystals	crystal	NOUN
eurjchem-2064	90	11	.	.	PUNCT
eurjchem-2064	91	1	m.p	m.p	PROPN
eurjchem-2064	91	2	.	.	PROPN
eurjchem-2064	91	3	:	:	PUNCT
eurjchem-2064	92	1	67	67	NUM
eurjchem-2064	92	2	-	-	SYM
eurjchem-2064	92	3	71	71	NUM
eurjchem-2064	92	4	°	°	NUM
eurjchem-2064	92	5	c	c	NOUN
eurjchem-2064	92	6	.	.	PUNCT
eurjchem-2064	93	1	rf	rf	VERB
eurjchem-2064	93	2	=	=	NOUN
eurjchem-2064	93	3	0.52	0.52	NUM
eurjchem-2064	93	4	(	(	PUNCT
eurjchem-2064	93	5	ch2cl2	ch2cl2	NOUN
eurjchem-2064	93	6	)	)	PUNCT
eurjchem-2064	93	7	.	.	PUNCT
eurjchem-2064	94	1	1h	1h	NUM
eurjchem-2064	94	2	nmr	nmr	NOUN
eurjchem-2064	94	3	(	(	PUNCT
eurjchem-2064	94	4	400	400	NUM
eurjchem-2064	94	5	mhz	mhz	NOUN
eurjchem-2064	94	6	,	,	PUNCT
eurjchem-2064	94	7	chloroform	chloroform	NOUN
eurjchem-2064	94	8	-	-	PUNCT
eurjchem-2064	94	9	d	d	PROPN
eurjchem-2064	94	10	,	,	PUNCT
eurjchem-2064	94	11	δ	δ	PROPN
eurjchem-2064	94	12	,	,	PUNCT
eurjchem-2064	94	13	ppm	ppm	NOUN
eurjchem-2064	94	14	):	):	PUNCT
eurjchem-2064	94	15	7.75	7.75	NUM
eurjchem-2064	94	16	(	(	PUNCT
eurjchem-2064	94	17	d	d	PROPN
eurjchem-2064	94	18	,	,	PUNCT
eurjchem-2064	94	19	j	j	PROPN
eurjchem-2064	94	20	=	=	SYM
eurjchem-2064	94	21	8.0	8.0	NUM
eurjchem-2064	94	22	hz	hz	NOUN
eurjchem-2064	94	23	,	,	PUNCT
eurjchem-2064	94	24	2h	2h	NUM
eurjchem-2064	94	25	)	)	PUNCT
eurjchem-2064	94	26	,	,	PUNCT
eurjchem-2064	94	27	7.30	7.30	NUM
eurjchem-2064	94	28	(	(	PUNCT
eurjchem-2064	94	29	d	d	PROPN
eurjchem-2064	94	30	,	,	PUNCT
eurjchem-2064	94	31	j	j	PROPN
eurjchem-2064	95	1	=	=	SYM
eurjchem-2064	95	2	8.0	8.0	NUM
eurjchem-2064	95	3	hz	hz	NOUN
eurjchem-2064	95	4	,	,	PUNCT
eurjchem-2064	95	5	2h	2h	NUM
eurjchem-2064	95	6	)	)	PUNCT
eurjchem-2064	95	7	,	,	PUNCT
eurjchem-2064	95	8	5.65	5.65	NUM
eurjchem-2064	95	9	-	-	SYM
eurjchem-2064	95	10	5.78	5.78	NUM
eurjchem-2064	95	11	(	(	PUNCT
eurjchem-2064	95	12	m	m	PROPN
eurjchem-2064	95	13	,	,	PUNCT
eurjchem-2064	95	14	1h	1h	NUM
eurjchem-2064	95	15	)	)	PUNCT
eurjchem-2064	95	16	,	,	PUNCT
eurjchem-2064	95	17	5.05	5.05	NUM
eurjchem-2064	95	18	-	-	SYM
eurjchem-2064	95	19	5.19	5.19	NUM
eurjchem-2064	95	20	(	(	PUNCT
eurjchem-2064	95	21	m	m	PROPN
eurjchem-2064	95	22	,	,	PUNCT
eurjchem-2064	95	23	2h	2h	NUM
eurjchem-2064	95	24	)	)	PUNCT
eurjchem-2064	95	25	,	,	PUNCT
eurjchem-2064	95	26	4.37	4.37	NUM
eurjchem-2064	95	27	(	(	PUNCT
eurjchem-2064	95	28	s	s	PROPN
eurjchem-2064	95	29	,	,	PUNCT
eurjchem-2064	95	30	1h	1h	NUM
eurjchem-2064	95	31	)	)	PUNCT
eurjchem-2064	95	32	,	,	PUNCT
eurjchem-2064	95	33	3.553.61	3.553.61	NUM
eurjchem-2064	95	34	(	(	PUNCT
eurjchem-2064	95	35	m	m	PROPN
eurjchem-2064	95	36	,	,	PUNCT
eurjchem-2064	95	37	2h	2h	NUM
eurjchem-2064	95	38	)	)	PUNCT
eurjchem-2064	95	39	,	,	PUNCT
eurjchem-2064	95	40	2.41	2.41	NUM
eurjchem-2064	95	41	(	(	PUNCT
eurjchem-2064	95	42	s	s	PROPN
eurjchem-2064	95	43	,	,	PUNCT
eurjchem-2064	95	44	3h	3h	NUM
eurjchem-2064	95	45	)	)	PUNCT
eurjchem-2064	95	46	.	.	PUNCT
eurjchem-2064	96	1	13c	13c	NOUN
eurjchem-2064	96	2	nmr	nmr	NOUN
eurjchem-2064	96	3	(	(	PUNCT
eurjchem-2064	96	4	100	100	NUM
eurjchem-2064	96	5	mhz	mhz	NOUN
eurjchem-2064	96	6	,	,	PUNCT
eurjchem-2064	96	7	chloroform	chloroform	NOUN
eurjchem-2064	96	8	-	-	PUNCT
eurjchem-2064	96	9	d	d	PROPN
eurjchem-2064	96	10	,	,	PUNCT
eurjchem-2064	96	11	δ	δ	PROPN
eurjchem-2064	96	12	,	,	PUNCT
eurjchem-2064	96	13	ppm	ppm	NOUN
eurjchem-2064	96	14	):	):	PUNCT
eurjchem-2064	96	15	143.66	143.66	NUM
eurjchem-2064	96	16	,	,	PUNCT
eurjchem-2064	96	17	136.98	136.98	NUM
eurjchem-2064	96	18	,	,	PUNCT
eurjchem-2064	96	19	133.06	133.06	NUM
eurjchem-2064	96	20	,	,	PUNCT
eurjchem-2064	96	21	129.85	129.85	NUM
eurjchem-2064	96	22	,	,	PUNCT
eurjchem-2064	96	23	127.25	127.25	NUM
eurjchem-2064	96	24	,	,	PUNCT
eurjchem-2064	96	25	117.87	117.87	NUM
eurjchem-2064	96	26	,	,	PUNCT
eurjchem-2064	96	27	45.90	45.90	NUM
eurjchem-2064	96	28	,	,	PUNCT
eurjchem-2064	96	29	21.65	21.65	NUM
eurjchem-2064	96	30	.	.	PUNCT
eurjchem-2064	96	31	4	4	NUM
eurjchem-2064	96	32	-	-	PUNCT
eurjchem-2064	96	33	methyl	methyl	NOUN
eurjchem-2064	96	34	-	-	PUNCT
eurjchem-2064	96	35	n-(4	n-(4	NOUN
eurjchem-2064	96	36	-	-	PUNCT
eurjchem-2064	96	37	methylbenzyl)benzenesulfonamide	methylbenzyl)benzenesulfonamide	NOUN
eurjchem-2064	96	38	(	(	PUNCT
eurjchem-2064	96	39	8)	8)	NUM
eurjchem-2064	96	40	:	:	PUNCT
eurjchem-2064	96	41	white	white	ADJ
eurjchem-2064	96	42	crystals	crystal	NOUN
eurjchem-2064	96	43	.	.	PUNCT
eurjchem-2064	97	1	m.p	m.p	PROPN
eurjchem-2064	97	2	.	.	PROPN
eurjchem-2064	97	3	:	:	PUNCT
eurjchem-2064	98	1	103	103	NUM
eurjchem-2064	98	2	-	-	SYM
eurjchem-2064	98	3	105	105	NUM
eurjchem-2064	98	4	°	°	NOUN
eurjchem-2064	98	5	c	c	NOUN
eurjchem-2064	98	6	.	.	PUNCT
eurjchem-2064	99	1	rf	rf	NOUN
eurjchem-2064	99	2	=	=	NOUN
eurjchem-2064	99	3	0.35	0.35	NUM
eurjchem-2064	99	4	(	(	PUNCT
eurjchem-2064	99	5	ch2cl2	ch2cl2	NOUN
eurjchem-2064	99	6	)	)	PUNCT
eurjchem-2064	99	7	.	.	PUNCT
eurjchem-2064	100	1	1h	1h	NUM
eurjchem-2064	100	2	nmr	nmr	NOUN
eurjchem-2064	100	3	(	(	PUNCT
eurjchem-2064	100	4	400	400	NUM
eurjchem-2064	100	5	mhz	mhz	NOUN
eurjchem-2064	100	6	,	,	PUNCT
eurjchem-2064	100	7	chloroform	chloroform	NOUN
eurjchem-2064	100	8	-	-	PUNCT
eurjchem-2064	100	9	d	d	PROPN
eurjchem-2064	100	10	,	,	PUNCT
eurjchem-2064	100	11	δ	δ	PROPN
eurjchem-2064	100	12	,	,	PUNCT
eurjchem-2064	100	13	ppm	ppm	NUM
eurjchem-2064	100	14	):	):	PUNCT
eurjchem-2064	100	15	7.74	7.74	NUM
eurjchem-2064	100	16	(	(	PUNCT
eurjchem-2064	100	17	d	d	PROPN
eurjchem-2064	100	18	,	,	PUNCT
eurjchem-2064	100	19	j	j	PROPN
eurjchem-2064	100	20	=	=	SYM
eurjchem-2064	100	21	8.1	8.1	NUM
eurjchem-2064	100	22	hz	hz	NOUN
eurjchem-2064	100	23	,	,	PUNCT
eurjchem-2064	100	24	2h	2h	NUM
eurjchem-2064	100	25	)	)	PUNCT
eurjchem-2064	100	26	,	,	PUNCT
eurjchem-2064	100	27	7.29	7.29	NUM
eurjchem-2064	100	28	(	(	PUNCT
eurjchem-2064	100	29	d	d	PROPN
eurjchem-2064	100	30	,	,	PUNCT
eurjchem-2064	100	31	j	j	PROPN
eurjchem-2064	101	1	=	=	SYM
eurjchem-2064	101	2	8.0	8.0	NUM
eurjchem-2064	101	3	hz	hz	NOUN
eurjchem-2064	101	4	,	,	PUNCT
eurjchem-2064	101	5	2h	2h	NUM
eurjchem-2064	101	6	)	)	PUNCT
eurjchem-2064	101	7	,	,	PUNCT
eurjchem-2064	101	8	7.06	7.06	NUM
eurjchem-2064	101	9	(	(	PUNCT
eurjchem-2064	101	10	s	s	PROPN
eurjchem-2064	101	11	,	,	PUNCT
eurjchem-2064	101	12	4h	4h	NOUN
eurjchem-2064	101	13	)	)	PUNCT
eurjchem-2064	101	14	,	,	PUNCT
eurjchem-2064	101	15	4.72	4.72	NUM
eurjchem-2064	101	16	-	-	SYM
eurjchem-2064	101	17	4.61	4.61	NUM
eurjchem-2064	101	18	(	(	PUNCT
eurjchem-2064	101	19	m	m	PROPN
eurjchem-2064	101	20	,	,	PUNCT
eurjchem-2064	101	21	1h	1h	NUM
eurjchem-2064	101	22	)	)	PUNCT
eurjchem-2064	101	23	,	,	PUNCT
eurjchem-2064	101	24	4.05	4.05	NUM
eurjchem-2064	101	25	(	(	PUNCT
eurjchem-2064	101	26	d	d	NOUN
eurjchem-2064	101	27	,	,	PUNCT
eurjchem-2064	101	28	j	j	PROPN
eurjchem-2064	101	29	=	=	SYM
eurjchem-2064	101	30	6.1	6.1	NUM
eurjchem-2064	101	31	hz	hz	NOUN
eurjchem-2064	101	32	,	,	PUNCT
eurjchem-2064	101	33	2h	2h	NUM
eurjchem-2064	101	34	)	)	PUNCT
eurjchem-2064	101	35	,	,	PUNCT
eurjchem-2064	101	36	2.43	2.43	NUM
eurjchem-2064	101	37	(	(	PUNCT
eurjchem-2064	101	38	s	s	PROPN
eurjchem-2064	101	39	,	,	PUNCT
eurjchem-2064	101	40	3h	3h	NUM
eurjchem-2064	101	41	)	)	PUNCT
eurjchem-2064	101	42	,	,	PUNCT
eurjchem-2064	101	43	2.29	2.29	NUM
eurjchem-2064	101	44	(	(	PUNCT
eurjchem-2064	101	45	s	s	PROPN
eurjchem-2064	101	46	,	,	PUNCT
eurjchem-2064	101	47	3h	3h	NUM
eurjchem-2064	101	48	)	)	PUNCT
eurjchem-2064	101	49	.	.	PUNCT
eurjchem-2064	102	1	13c	13c	NOUN
eurjchem-2064	102	2	nmr	nmr	NOUN
eurjchem-2064	102	3	(	(	PUNCT
eurjchem-2064	102	4	100	100	NUM
eurjchem-2064	102	5	mhz	mhz	NOUN
eurjchem-2064	102	6	,	,	PUNCT
eurjchem-2064	102	7	chloroform	chloroform	NOUN
eurjchem-2064	102	8	-	-	PUNCT
eurjchem-2064	102	9	d	d	PROPN
eurjchem-2064	102	10	,	,	PUNCT
eurjchem-2064	102	11	δ	δ	PROPN
eurjchem-2064	102	12	,	,	PUNCT
eurjchem-2064	102	13	ppm	ppm	NOUN
eurjchem-2064	102	14	):	):	PUNCT
eurjchem-2064	102	15	143.60	143.60	NUM
eurjchem-2064	102	16	,	,	PUNCT
eurjchem-2064	102	17	137.80	137.80	NUM
eurjchem-2064	102	18	,	,	PUNCT
eurjchem-2064	102	19	136.90	136.90	NUM
eurjchem-2064	102	20	,	,	PUNCT
eurjchem-2064	102	21	133.28	133.28	NUM
eurjchem-2064	102	22	,	,	PUNCT
eurjchem-2064	102	23	129.84	129.84	NUM
eurjchem-2064	102	24	,	,	PUNCT
eurjchem-2064	102	25	129.46	129.46	NUM
eurjchem-2064	102	26	,	,	PUNCT
eurjchem-2064	102	27	127.97	127.97	NUM
eurjchem-2064	102	28	,	,	PUNCT
eurjchem-2064	102	29	127.31	127.31	NUM
eurjchem-2064	102	30	,	,	PUNCT
eurjchem-2064	102	31	47.15	47.15	NUM
eurjchem-2064	102	32	,	,	PUNCT
eurjchem-2064	102	33	21.66	21.66	NUM
eurjchem-2064	102	34	,	,	PUNCT
eurjchem-2064	102	35	21.19	21.19	NUM
eurjchem-2064	102	36	.	.	PUNCT
eurjchem-2064	102	37	4	4	NUM
eurjchem-2064	102	38	-	-	PUNCT
eurjchem-2064	102	39	methyl	methyl	NOUN
eurjchem-2064	102	40	-	-	PUNCT
eurjchem-2064	102	41	n	n	CCONJ
eurjchem-2064	102	42	-	-	PUNCT
eurjchem-2064	102	43	phenylbenzenesulfonamide	phenylbenzenesulfonamide	NOUN
eurjchem-2064	102	44	(	(	PUNCT
eurjchem-2064	102	45	9	9	NUM
eurjchem-2064	102	46	):	):	PUNCT
eurjchem-2064	102	47	pale	pale	ADJ
eurjchem-2064	102	48	-	-	PUNCT
eurjchem-2064	102	49	pink	pink	ADJ
eurjchem-2064	102	50	crystals	crystal	NOUN
eurjchem-2064	102	51	.	.	PUNCT
eurjchem-2064	103	1	m.p	m.p	PROPN
eurjchem-2064	103	2	.	.	PROPN
eurjchem-2064	103	3	:	:	PUNCT
eurjchem-2064	104	1	110	110	NUM
eurjchem-2064	104	2	-	-	SYM
eurjchem-2064	104	3	114	114	NUM
eurjchem-2064	104	4	°	°	NUM
eurjchem-2064	104	5	c	c	NOUN
eurjchem-2064	104	6	.	.	PUNCT
eurjchem-2064	105	1	rf	rf	NOUN
eurjchem-2064	105	2	=	=	NOUN
eurjchem-2064	105	3	0.36	0.36	NUM
eurjchem-2064	105	4	(	(	PUNCT
eurjchem-2064	105	5	ch2cl2	ch2cl2	NOUN
eurjchem-2064	105	6	)	)	PUNCT
eurjchem-2064	105	7	.	.	PUNCT
eurjchem-2064	106	1	1h	1h	NUM
eurjchem-2064	106	2	nmr	nmr	NOUN
eurjchem-2064	106	3	(	(	PUNCT
eurjchem-2064	106	4	400	400	NUM
eurjchem-2064	106	5	mhz	mhz	NOUN
eurjchem-2064	106	6	,	,	PUNCT
eurjchem-2064	106	7	chloroform	chloroform	NOUN
eurjchem-2064	106	8	-	-	PUNCT
eurjchem-2064	106	9	d	d	PROPN
eurjchem-2064	106	10	,	,	PUNCT
eurjchem-2064	106	11	δ	δ	PROPN
eurjchem-2064	106	12	,	,	PUNCT
eurjchem-2064	106	13	ppm	ppm	NUM
eurjchem-2064	106	14	):	):	PUNCT
eurjchem-2064	106	15	7.63	7.63	NUM
eurjchem-2064	106	16	(	(	PUNCT
eurjchem-2064	106	17	d	d	PROPN
eurjchem-2064	106	18	,	,	PUNCT
eurjchem-2064	106	19	j	j	PROPN
eurjchem-2064	106	20	=	=	PROPN
eurjchem-2064	106	21	8.00	8.00	NUM
eurjchem-2064	106	22	hz	hz	VERB
eurjchem-2064	106	23	,	,	PUNCT
eurjchem-2064	106	24	2h	2h	NUM
eurjchem-2064	106	25	)	)	PUNCT
eurjchem-2064	106	26	,	,	PUNCT
eurjchem-2064	106	27	7.18	7.18	NUM
eurjchem-2064	106	28	-	-	SYM
eurjchem-2064	106	29	7.27	7.27	NUM
eurjchem-2064	106	30	(	(	PUNCT
eurjchem-2064	106	31	m	m	PROPN
eurjchem-2064	106	32	,	,	PUNCT
eurjchem-2064	106	33	4h	4h	NOUN
eurjchem-2064	106	34	)	)	PUNCT
eurjchem-2064	106	35	,	,	PUNCT
eurjchem-2064	106	36	7.01	7.01	NUM
eurjchem-2064	106	37	-	-	SYM
eurjchem-2064	106	38	7.12	7.12	NUM
eurjchem-2064	106	39	(	(	PUNCT
eurjchem-2064	106	40	m	m	PROPN
eurjchem-2064	106	41	,	,	PUNCT
eurjchem-2064	106	42	3h	3h	NUM
eurjchem-2064	106	43	)	)	PUNCT
eurjchem-2064	106	44	,	,	PUNCT
eurjchem-2064	106	45	6.63	6.63	NUM
eurjchem-2064	106	46	(	(	PUNCT
eurjchem-2064	106	47	s	s	PROPN
eurjchem-2064	106	48	,	,	PUNCT
eurjchem-2064	106	49	1h	1h	NUM
eurjchem-2064	106	50	)	)	PUNCT
eurjchem-2064	106	51	,	,	PUNCT
eurjchem-2064	106	52	2.38	2.38	NUM
eurjchem-2064	106	53	(	(	PUNCT
eurjchem-2064	106	54	s	s	PROPN
eurjchem-2064	106	55	,	,	PUNCT
eurjchem-2064	106	56	3h	3h	NUM
eurjchem-2064	106	57	)	)	PUNCT
eurjchem-2064	106	58	.	.	PUNCT
eurjchem-2064	107	1	13c	13c	NOUN
eurjchem-2064	107	2	nmr	nmr	NOUN
eurjchem-2064	107	3	(	(	PUNCT
eurjchem-2064	107	4	100	100	NUM
eurjchem-2064	107	5	mhz	mhz	NOUN
eurjchem-2064	107	6	,	,	PUNCT
eurjchem-2064	107	7	chloroform	chloroform	NOUN
eurjchem-2064	107	8	-	-	PUNCT
eurjchem-2064	107	9	d	d	PROPN
eurjchem-2064	107	10	,	,	PUNCT
eurjchem-2064	107	11	δ	δ	PROPN
eurjchem-2064	107	12	,	,	PUNCT
eurjchem-2064	107	13	ppm	ppm	NOUN
eurjchem-2064	107	14	):	):	PUNCT
eurjchem-2064	107	15	144.01	144.01	NUM
eurjchem-2064	107	16	,	,	PUNCT
eurjchem-2064	107	17	136.61	136.61	NUM
eurjchem-2064	107	18	,	,	PUNCT
eurjchem-2064	107	19	136.07	136.07	NUM
eurjchem-2064	107	20	,	,	PUNCT
eurjchem-2064	107	21	129.76	129.76	NUM
eurjchem-2064	107	22	,	,	PUNCT
eurjchem-2064	107	23	129.41	129.41	NUM
eurjchem-2064	107	24	,	,	PUNCT
eurjchem-2064	107	25	127.38	127.38	NUM
eurjchem-2064	107	26	,	,	PUNCT
eurjchem-2064	107	27	125.40	125.40	NUM
eurjchem-2064	107	28	,	,	PUNCT
eurjchem-2064	107	29	121.62	121.62	NUM
eurjchem-2064	107	30	,	,	PUNCT
eurjchem-2064	107	31	21.65	21.65	NUM
eurjchem-2064	107	32	.	.	PUNCT
eurjchem-2064	107	33	4	4	NUM
eurjchem-2064	107	34	-	-	PUNCT
eurjchem-2064	107	35	methyl	methyl	NOUN
eurjchem-2064	107	36	-	-	PUNCT
eurjchem-2064	107	37	n	n	CCONJ
eurjchem-2064	107	38	-	-	PUNCT
eurjchem-2064	107	39	propylbenzenesulfonamide	propylbenzenesulfonamide	NOUN
eurjchem-2064	107	40	(	(	PUNCT
eurjchem-2064	107	41	10	10	NUM
eurjchem-2064	107	42	):	):	PUNCT
eurjchem-2064	107	43	transparent	transparent	ADJ
eurjchem-2064	107	44	crystals	crystal	NOUN
eurjchem-2064	107	45	.	.	PUNCT
eurjchem-2064	108	1	m.p	m.p	PROPN
eurjchem-2064	108	2	.	.	PROPN
eurjchem-2064	108	3	:	:	PUNCT
eurjchem-2064	109	1	61.5	61.5	NUM
eurjchem-2064	109	2	-	-	SYM
eurjchem-2064	109	3	63	63	NUM
eurjchem-2064	109	4	°	°	NOUN
eurjchem-2064	109	5	c	c	NOUN
eurjchem-2064	109	6	.	.	PUNCT
eurjchem-2064	110	1	rf	rf	VERB
eurjchem-2064	110	2	=	=	NOUN
eurjchem-2064	110	3	0.52	0.52	NUM
eurjchem-2064	110	4	(	(	PUNCT
eurjchem-2064	110	5	ch2cl2	ch2cl2	NOUN
eurjchem-2064	110	6	)	)	PUNCT
eurjchem-2064	110	7	.	.	PUNCT
eurjchem-2064	111	1	1h	1h	NUM
eurjchem-2064	111	2	nmr	nmr	NOUN
eurjchem-2064	111	3	(	(	PUNCT
eurjchem-2064	111	4	400	400	NUM
eurjchem-2064	111	5	mhz	mhz	NOUN
eurjchem-2064	111	6	,	,	PUNCT
eurjchem-2064	111	7	chloroform	chloroform	NOUN
eurjchem-2064	111	8	-	-	PUNCT
eurjchem-2064	111	9	d	d	PROPN
eurjchem-2064	111	10	,	,	PUNCT
eurjchem-2064	111	11	δ	δ	PROPN
eurjchem-2064	111	12	,	,	PUNCT
eurjchem-2064	111	13	ppm	ppm	NOUN
eurjchem-2064	111	14	):	):	PUNCT
eurjchem-2064	111	15	7.75	7.75	NUM
eurjchem-2064	111	16	(	(	PUNCT
eurjchem-2064	111	17	d	d	PROPN
eurjchem-2064	111	18	,	,	PUNCT
eurjchem-2064	111	19	j	j	PROPN
eurjchem-2064	111	20	=	=	PROPN
eurjchem-2064	111	21	8.2	8.2	NUM
eurjchem-2064	111	22	hz	hz	NOUN
eurjchem-2064	111	23	,	,	PUNCT
eurjchem-2064	111	24	2h	2h	NUM
eurjchem-2064	111	25	)	)	PUNCT
eurjchem-2064	111	26	,	,	PUNCT
eurjchem-2064	111	27	7.31	7.31	NUM
eurjchem-2064	111	28	(	(	PUNCT
eurjchem-2064	111	29	d	d	NOUN
eurjchem-2064	111	30	,	,	PUNCT
eurjchem-2064	111	31	j	j	PROPN
eurjchem-2064	112	1	=	=	PROPN
eurjchem-2064	112	2	8.2	8.2	NUM
eurjchem-2064	112	3	hz	hz	NOUN
eurjchem-2064	112	4	,	,	PUNCT
eurjchem-2064	112	5	2h	2h	NUM
eurjchem-2064	112	6	)	)	PUNCT
eurjchem-2064	112	7	,	,	PUNCT
eurjchem-2064	112	8	4.39	4.39	NUM
eurjchem-2064	112	9	(	(	PUNCT
eurjchem-2064	112	10	s	s	PROPN
eurjchem-2064	112	11	,	,	PUNCT
eurjchem-2064	112	12	1h	1h	NUM
eurjchem-2064	112	13	)	)	PUNCT
eurjchem-2064	112	14	,	,	PUNCT
eurjchem-2064	112	15	2.89	2.89	NUM
eurjchem-2064	112	16	(	(	PUNCT
eurjchem-2064	112	17	q	q	NOUN
eurjchem-2064	112	18	,	,	PUNCT
eurjchem-2064	112	19	j	j	PROPN
eurjchem-2064	112	20	=	=	SYM
eurjchem-2064	112	21	6.8	6.8	NUM
eurjchem-2064	112	22	hz	hz	NOUN
eurjchem-2064	112	23	,	,	PUNCT
eurjchem-2064	112	24	2h	2h	NUM
eurjchem-2064	112	25	)	)	PUNCT
eurjchem-2064	112	26	,	,	PUNCT
eurjchem-2064	112	27	2.41	2.41	NUM
eurjchem-2064	112	28	(	(	PUNCT
eurjchem-2064	112	29	s	s	PROPN
eurjchem-2064	112	30	,	,	PUNCT
eurjchem-2064	112	31	3h	3h	NUM
eurjchem-2064	112	32	)	)	PUNCT
eurjchem-2064	112	33	,	,	PUNCT
eurjchem-2064	112	34	1.401.51	1.401.51	NUM
eurjchem-2064	112	35	(	(	PUNCT
eurjchem-2064	112	36	m	m	PROPN
eurjchem-2064	112	37	,	,	PUNCT
eurjchem-2064	112	38	2h	2h	NUM
eurjchem-2064	112	39	)	)	PUNCT
eurjchem-2064	112	40	,	,	PUNCT
eurjchem-2064	112	41	0.95	0.95	NUM
eurjchem-2064	112	42	(	(	PUNCT
eurjchem-2064	112	43	t	t	PROPN
eurjchem-2064	112	44	,	,	PUNCT
eurjchem-2064	112	45	j	j	PROPN
eurjchem-2064	113	1	=	=	SYM
eurjchem-2064	113	2	6.0	6.0	NUM
eurjchem-2064	113	3	hz	hz	NOUN
eurjchem-2064	113	4	,	,	PUNCT
eurjchem-2064	113	5	3h	3h	NUM
eurjchem-2064	113	6	)	)	PUNCT
eurjchem-2064	113	7	.	.	PUNCT
eurjchem-2064	114	1	13c	13c	NOUN
eurjchem-2064	114	2	nmr	nmr	NOUN
eurjchem-2064	114	3	(	(	PUNCT
eurjchem-2064	114	4	100	100	NUM
eurjchem-2064	114	5	mhz	mhz	NOUN
eurjchem-2064	114	6	,	,	PUNCT
eurjchem-2064	114	7	chloroform	chloroform	NOUN
eurjchem-2064	114	8	-	-	PUNCT
eurjchem-2064	114	9	d	d	PROPN
eurjchem-2064	114	10	,	,	PUNCT
eurjchem-2064	114	11	δ	δ	PROPN
eurjchem-2064	114	12	,	,	PUNCT
eurjchem-2064	114	13	ppm	ppm	NUM
eurjchem-2064	114	14	):	):	PUNCT
eurjchem-2064	114	15	143.46	143.46	NUM
eurjchem-2064	114	16	,	,	PUNCT
eurjchem-2064	114	17	137.07	137.07	NUM
eurjchem-2064	114	18	,	,	PUNCT
eurjchem-2064	114	19	129.80	129.80	NUM
eurjchem-2064	114	20	,	,	PUNCT
eurjchem-2064	114	21	127.19	127.19	NUM
eurjchem-2064	114	22	,	,	PUNCT
eurjchem-2064	114	23	45.05	45.05	NUM
eurjchem-2064	114	24	,	,	PUNCT
eurjchem-2064	114	25	23.04	23.04	NUM
eurjchem-2064	114	26	,	,	PUNCT
eurjchem-2064	114	27	21.63	21.63	NUM
eurjchem-2064	114	28	,	,	PUNCT
eurjchem-2064	114	29	11.20	11.20	NUM
eurjchem-2064	114	30	.	.	PUNCT
eurjchem-2064	115	1	2.1.2	2.1.2	NUM
eurjchem-2064	115	2	.	.	PUNCT
eurjchem-2064	115	3	general	general	ADJ
eurjchem-2064	115	4	procedure	procedure	NOUN
eurjchem-2064	115	5	for	for	ADP
eurjchem-2064	115	6	the	the	DET
eurjchem-2064	115	7	preparation	preparation	NOUN
eurjchem-2064	115	8	of	of	ADP
eurjchem-2064	115	9	sulfonamides	sulfonamide	NOUN
eurjchem-2064	115	10	synthesized	synthesize	VERB
eurjchem-2064	115	11	in	in	ADP
eurjchem-2064	115	12	the	the	DET
eurjchem-2064	115	13	presence	presence	NOUN
eurjchem-2064	115	14	of	of	ADP
eurjchem-2064	115	15	potassium	potassium	NOUN
eurjchem-2064	115	16	carbonate	carbonate	NOUN
eurjchem-2064	115	17	(	(	PUNCT
eurjchem-2064	115	18	1	1	NUM
eurjchem-2064	115	19	-	-	SYM
eurjchem-2064	115	20	13	13	NUM
eurjchem-2064	115	21	)	)	PUNCT
eurjchem-2064	115	22	4	4	NUM
eurjchem-2064	115	23	-	-	PUNCT
eurjchem-2064	115	24	methylbenzenesulfonyl	methylbenzenesulfonyl	NOUN
eurjchem-2064	115	25	chloride	chloride	NOUN
eurjchem-2064	115	26	(	(	PUNCT
eurjchem-2064	115	27	1.00	1.00	NUM
eurjchem-2064	115	28	g	g	NOUN
eurjchem-2064	115	29	,	,	PUNCT
eurjchem-2064	115	30	5.25	5.25	NUM
eurjchem-2064	115	31	mmol	mmol	NOUN
eurjchem-2064	115	32	)	)	PUNCT
eurjchem-2064	115	33	was	be	AUX
eurjchem-2064	115	34	added	add	VERB
eurjchem-2064	115	35	to	to	ADP
eurjchem-2064	115	36	a	a	DET
eurjchem-2064	115	37	flask	flask	NOUN
eurjchem-2064	115	38	containing	contain	VERB
eurjchem-2064	115	39	10	10	NUM
eurjchem-2064	115	40	ml	ml	NOUN
eurjchem-2064	115	41	of	of	ADP
eurjchem-2064	115	42	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-2064	115	43	.	.	PUNCT
eurjchem-2064	116	1	an	an	DET
eurjchem-2064	116	2	amine	amine	ADJ
eurjchem-2064	116	3	(	(	PUNCT
eurjchem-2064	116	4	5.90	5.90	NUM
eurjchem-2064	116	5	mmol	mmol	NOUN
eurjchem-2064	116	6	)	)	PUNCT
eurjchem-2064	116	7	was	be	AUX
eurjchem-2064	116	8	added	add	VERB
eurjchem-2064	116	9	dropwise	dropwise	NOUN
eurjchem-2064	116	10	to	to	ADP
eurjchem-2064	116	11	the	the	DET
eurjchem-2064	116	12	stirring	stirring	ADJ
eurjchem-2064	116	13	solution	solution	NOUN
eurjchem-2064	116	14	,	,	PUNCT
eurjchem-2064	116	15	followed	follow	VERB
eurjchem-2064	116	16	by	by	ADP
eurjchem-2064	116	17	the	the	DET
eurjchem-2064	116	18	dropwise	dropwise	NOUN
eurjchem-2064	116	19	addition	addition	NOUN
eurjchem-2064	116	20	of	of	ADP
eurjchem-2064	116	21	0.59	0.59	NUM
eurjchem-2064	116	22	m	m	NOUN
eurjchem-2064	116	23	aqueous	aqueous	ADJ
eurjchem-2064	116	24	potassium	potassium	NOUN
eurjchem-2064	116	25	carbonate	carbonate	NOUN
eurjchem-2064	116	26	(	(	PUNCT
eurjchem-2064	116	27	10	10	NUM
eurjchem-2064	116	28	ml	ml	NOUN
eurjchem-2064	116	29	,	,	PUNCT
eurjchem-2064	116	30	5.90	5.90	NUM
eurjchem-2064	116	31	mmol	mmol	NOUN
eurjchem-2064	116	32	)	)	PUNCT
eurjchem-2064	116	33	.	.	PUNCT
eurjchem-2064	117	1	the	the	DET
eurjchem-2064	117	2	flask	flask	NOUN
eurjchem-2064	117	3	was	be	AUX
eurjchem-2064	117	4	sealed	seal	VERB
eurjchem-2064	117	5	and	and	CCONJ
eurjchem-2064	117	6	left	leave	VERB
eurjchem-2064	117	7	to	to	PART
eurjchem-2064	117	8	react	react	VERB
eurjchem-2064	117	9	to	to	ADP
eurjchem-2064	117	10	completion	completion	NOUN
eurjchem-2064	117	11	at	at	ADP
eurjchem-2064	117	12	room	room	NOUN
eurjchem-2064	117	13	temperature	temperature	NOUN
eurjchem-2064	117	14	.	.	PUNCT
eurjchem-2064	118	1	reaction	reaction	NOUN
eurjchem-2064	118	2	completion	completion	NOUN
eurjchem-2064	118	3	was	be	AUX
eurjchem-2064	118	4	verified	verify	VERB
eurjchem-2064	118	5	by	by	ADP
eurjchem-2064	118	6	tlc	tlc	NOUN
eurjchem-2064	118	7	analysis	analysis	NOUN
eurjchem-2064	118	8	.	.	PUNCT
eurjchem-2064	119	1	the	the	DET
eurjchem-2064	119	2	mixture	mixture	NOUN
eurjchem-2064	119	3	was	be	AUX
eurjchem-2064	119	4	then	then	ADV
eurjchem-2064	119	5	concentrated	concentrate	VERB
eurjchem-2064	119	6	to	to	ADP
eurjchem-2064	119	7	half	half	DET
eurjchem-2064	119	8	its	its	PRON
eurjchem-2064	119	9	volume	volume	NOUN
eurjchem-2064	119	10	,	,	PUNCT
eurjchem-2064	119	11	acidified	acidify	VERB
eurjchem-2064	119	12	with	with	ADP
eurjchem-2064	119	13	5	5	NUM
eurjchem-2064	119	14	m	m	NOUN
eurjchem-2064	119	15	hcl	hcl	NOUN
eurjchem-2064	119	16	,	,	PUNCT
eurjchem-2064	119	17	and	and	CCONJ
eurjchem-2064	119	18	chilled	chill	VERB
eurjchem-2064	119	19	.	.	PUNCT
eurjchem-2064	120	1	the	the	DET
eurjchem-2064	120	2	resulting	result	VERB
eurjchem-2064	120	3	precipitate	precipitate	NOUN
eurjchem-2064	120	4	is	be	AUX
eurjchem-2064	120	5	isolated	isolate	VERB
eurjchem-2064	120	6	via	via	ADP
eurjchem-2064	120	7	vacuum	vacuum	NOUN
eurjchem-2064	120	8	filtration	filtration	NOUN
eurjchem-2064	120	9	and	and	CCONJ
eurjchem-2064	120	10	recrystallized	recrystallize	VERB
eurjchem-2064	120	11	from	from	ADP
eurjchem-2064	120	12	ethanol	ethanol	NOUN
eurjchem-2064	120	13	to	to	PART
eurjchem-2064	120	14	afford	afford	VERB
eurjchem-2064	120	15	the	the	DET
eurjchem-2064	120	16	product	product	NOUN
eurjchem-2064	120	17	in	in	ADP
eurjchem-2064	120	18	good	good	ADJ
eurjchem-2064	120	19	purity	purity	NOUN
eurjchem-2064	120	20	and	and	CCONJ
eurjchem-2064	120	21	yield	yield	NOUN
eurjchem-2064	120	22	.	.	PUNCT
eurjchem-2064	121	1	n	n	CCONJ
eurjchem-2064	121	2	,	,	PUNCT
eurjchem-2064	121	3	n	n	CCONJ
eurjchem-2064	121	4	-	-	PUNCT
eurjchem-2064	121	5	bis(2	bis(2	NOUN
eurjchem-2064	121	6	-	-	PUNCT
eurjchem-2064	121	7	hydroxyethyl)-4	hydroxyethyl)-4	NOUN
eurjchem-2064	121	8	-	-	PUNCT
eurjchem-2064	121	9	methylbenzenesulfonamide	methylbenzenesulfonamide	NOUN
eurjchem-2064	121	10	(	(	PUNCT
eurjchem-2064	121	11	11	11	NUM
eurjchem-2064	121	12	):	):	PUNCT
eurjchem-2064	121	13	white	white	ADJ
eurjchem-2064	121	14	crystals	crystal	NOUN
eurjchem-2064	121	15	.	.	PUNCT
eurjchem-2064	122	1	m.p	m.p	PROPN
eurjchem-2064	122	2	.	.	PROPN
eurjchem-2064	122	3	:	:	PUNCT
eurjchem-2064	122	4	85	85	NUM
eurjchem-2064	122	5	-	-	SYM
eurjchem-2064	122	6	87	87	NUM
eurjchem-2064	122	7	°	°	SYM
eurjchem-2064	122	8	c	c	NOUN
eurjchem-2064	122	9	.	.	PUNCT
eurjchem-2064	123	1	rf	rf	VERB
eurjchem-2064	123	2	=	=	NOUN
eurjchem-2064	123	3	0.11	0.11	NUM
eurjchem-2064	123	4	(	(	PUNCT
eurjchem-2064	123	5	ch2cl2	ch2cl2	NOUN
eurjchem-2064	123	6	)	)	PUNCT
eurjchem-2064	123	7	.	.	PUNCT
eurjchem-2064	124	1	1h	1h	NUM
eurjchem-2064	124	2	nmr	nmr	NOUN
eurjchem-2064	124	3	(	(	PUNCT
eurjchem-2064	124	4	400	400	NUM
eurjchem-2064	124	5	mhz	mhz	NOUN
eurjchem-2064	124	6	,	,	PUNCT
eurjchem-2064	124	7	chloroform	chloroform	NOUN
eurjchem-2064	124	8	-	-	PUNCT
eurjchem-2064	124	9	d	d	PROPN
eurjchem-2064	124	10	,	,	PUNCT
eurjchem-2064	124	11	δ	δ	PROPN
eurjchem-2064	124	12	,	,	PUNCT
eurjchem-2064	124	13	ppm	ppm	NUM
eurjchem-2064	124	14	):	):	PUNCT
eurjchem-2064	124	15	7.68	7.68	NUM
eurjchem-2064	124	16	(	(	PUNCT
eurjchem-2064	124	17	d	d	PROPN
eurjchem-2064	124	18	,	,	PUNCT
eurjchem-2064	124	19	j	j	PROPN
eurjchem-2064	124	20	=	=	SYM
eurjchem-2064	124	21	8.3	8.3	NUM
eurjchem-2064	124	22	hz	hz	NOUN
eurjchem-2064	124	23	,	,	PUNCT
eurjchem-2064	124	24	2h	2h	NUM
eurjchem-2064	124	25	)	)	PUNCT
eurjchem-2064	124	26	,	,	PUNCT
eurjchem-2064	124	27	7.31	7.31	NUM
eurjchem-2064	124	28	(	(	PUNCT
eurjchem-2064	124	29	d	d	NOUN
eurjchem-2064	124	30	,	,	PUNCT
eurjchem-2064	124	31	j	j	PROPN
eurjchem-2064	124	32	=	=	SYM
eurjchem-2064	124	33	8.0	8.0	NUM
eurjchem-2064	124	34	hz	hz	NOUN
eurjchem-2064	124	35	,	,	PUNCT
eurjchem-2064	124	36	2h	2h	NUM
eurjchem-2064	124	37	)	)	PUNCT
eurjchem-2064	124	38	,	,	PUNCT
eurjchem-2064	124	39	3.84	3.84	NUM
eurjchem-2064	124	40	(	(	PUNCT
eurjchem-2064	124	41	t	t	PROPN
eurjchem-2064	124	42	,	,	PUNCT
eurjchem-2064	124	43	j	j	PROPN
eurjchem-2064	125	1	=	=	SYM
eurjchem-2064	125	2	5.0	5.0	NUM
eurjchem-2064	125	3	hz	hz	NOUN
eurjchem-2064	125	4	,	,	PUNCT
eurjchem-2064	125	5	4h	4h	NOUN
eurjchem-2064	125	6	)	)	PUNCT
eurjchem-2064	125	7	,	,	PUNCT
eurjchem-2064	125	8	3.73	3.73	NUM
eurjchem-2064	125	9	(	(	PUNCT
eurjchem-2064	125	10	s	s	PROPN
eurjchem-2064	125	11	,	,	PUNCT
eurjchem-2064	125	12	1h	1h	NUM
eurjchem-2064	125	13	)	)	PUNCT
eurjchem-2064	125	14	,	,	PUNCT
eurjchem-2064	125	15	3.27	3.27	NUM
eurjchem-2064	125	16	-	-	SYM
eurjchem-2064	125	17	3.20	3.20	NUM
eurjchem-2064	125	18	(	(	PUNCT
eurjchem-2064	125	19	t	t	PROPN
eurjchem-2064	125	20	,	,	PUNCT
eurjchem-2064	125	21	j	j	PROPN
eurjchem-2064	125	22	=	=	SYM
eurjchem-2064	125	23	4.8	4.8	NUM
eurjchem-2064	125	24	hz	hz	NOUN
eurjchem-2064	125	25	,	,	PUNCT
eurjchem-2064	125	26	4h	4h	NOUN
eurjchem-2064	125	27	)	)	PUNCT
eurjchem-2064	125	28	,	,	PUNCT
eurjchem-2064	125	29	2.41	2.41	NUM
eurjchem-2064	125	30	(	(	PUNCT
eurjchem-2064	125	31	s	s	PROPN
eurjchem-2064	125	32	,	,	PUNCT
eurjchem-2064	125	33	3h	3h	NUM
eurjchem-2064	125	34	)	)	PUNCT
eurjchem-2064	125	35	.	.	PUNCT
eurjchem-2064	126	1	13c	13c	NOUN
eurjchem-2064	126	2	nmr	nmr	NOUN
eurjchem-2064	126	3	(	(	PUNCT
eurjchem-2064	126	4	100	100	NUM
eurjchem-2064	126	5	mhz	mhz	NOUN
eurjchem-2064	126	6	,	,	PUNCT
eurjchem-2064	126	7	chloroform	chloroform	NOUN
eurjchem-2064	126	8	-	-	PUNCT
eurjchem-2064	126	9	d	d	PROPN
eurjchem-2064	126	10	,	,	PUNCT
eurjchem-2064	126	11	δ	δ	PROPN
eurjchem-2064	126	12	,	,	PUNCT
eurjchem-2064	126	13	ppm	ppm	NOUN
eurjchem-2064	126	14	):	):	PUNCT
eurjchem-2064	126	15	143.89	143.89	NUM
eurjchem-2064	126	16	,	,	PUNCT
eurjchem-2064	126	17	135.29	135.29	NUM
eurjchem-2064	126	18	,	,	PUNCT
eurjchem-2064	126	19	129.97	129.97	NUM
eurjchem-2064	126	20	,	,	PUNCT
eurjchem-2064	126	21	127.41	127.41	NUM
eurjchem-2064	126	22	,	,	PUNCT
eurjchem-2064	126	23	62.46	62.46	NUM
eurjchem-2064	126	24	,	,	PUNCT
eurjchem-2064	126	25	53.06	53.06	NUM
eurjchem-2064	126	26	,	,	PUNCT
eurjchem-2064	126	27	21.64	21.64	NUM
eurjchem-2064	126	28	.	.	NOUN
eurjchem-2064	126	29	4	4	NUM
eurjchem-2064	126	30	-	-	PUNCT
eurjchem-2064	126	31	methyl	methyl	NOUN
eurjchem-2064	126	32	-	-	PUNCT
eurjchem-2064	126	33	n-(2	n-(2	NOUN
eurjchem-2064	126	34	,	,	PUNCT
eurjchem-2064	126	35	4	4	NUM
eurjchem-2064	126	36	,	,	PUNCT
eurjchem-2064	126	37	4	4	NUM
eurjchem-2064	126	38	-	-	PUNCT
eurjchem-2064	126	39	trimethylpentan-2	trimethylpentan-2	NUM
eurjchem-2064	126	40	-	-	PUNCT
eurjchem-2064	126	41	yl)benzenesulfonamide	yl)benzenesulfonamide	NOUN
eurjchem-2064	126	42	(	(	PUNCT
eurjchem-2064	126	43	12	12	NUM
eurjchem-2064	126	44	):	):	PUNCT
eurjchem-2064	126	45	white	white	ADJ
eurjchem-2064	126	46	crystals	crystal	NOUN
eurjchem-2064	126	47	.	.	PUNCT
eurjchem-2064	127	1	m.p	m.p	PROPN
eurjchem-2064	127	2	.	.	PROPN
eurjchem-2064	127	3	:	:	PUNCT
eurjchem-2064	128	1	142	142	NUM
eurjchem-2064	128	2	-	-	SYM
eurjchem-2064	128	3	145	145	NUM
eurjchem-2064	128	4	°	°	NUM
eurjchem-2064	128	5	c	c	NOUN
eurjchem-2064	128	6	.	.	PUNCT
eurjchem-2064	129	1	rf	rf	NOUN
eurjchem-2064	129	2	=	=	NOUN
eurjchem-2064	129	3	0.60	0.60	NUM
eurjchem-2064	129	4	(	(	PUNCT
eurjchem-2064	129	5	ch2cl2	ch2cl2	NOUN
eurjchem-2064	129	6	)	)	PUNCT
eurjchem-2064	129	7	.	.	PUNCT
eurjchem-2064	130	1	1h	1h	NUM
eurjchem-2064	130	2	nmr	nmr	NOUN
eurjchem-2064	130	3	(	(	PUNCT
eurjchem-2064	130	4	400	400	NUM
eurjchem-2064	130	5	mhz	mhz	NOUN
eurjchem-2064	130	6	,	,	PUNCT
eurjchem-2064	130	7	chloroform	chloroform	NOUN
eurjchem-2064	130	8	-	-	PUNCT
eurjchem-2064	130	9	d	d	PROPN
eurjchem-2064	130	10	,	,	PUNCT
eurjchem-2064	130	11	δ	δ	PROPN
eurjchem-2064	130	12	,	,	PUNCT
eurjchem-2064	130	13	ppm	ppm	NUM
eurjchem-2064	130	14	):	):	PUNCT
eurjchem-2064	130	15	7.79	7.79	NUM
eurjchem-2064	130	16	-	-	SYM
eurjchem-2064	130	17	7.71	7.71	NUM
eurjchem-2064	130	18	(	(	PUNCT
eurjchem-2064	130	19	m	m	PROPN
eurjchem-2064	130	20	,	,	PUNCT
eurjchem-2064	130	21	2h	2h	NUM
eurjchem-2064	130	22	)	)	PUNCT
eurjchem-2064	130	23	,	,	PUNCT
eurjchem-2064	130	24	7.25	7.25	NUM
eurjchem-2064	130	25	(	(	PUNCT
eurjchem-2064	130	26	d	d	PROPN
eurjchem-2064	130	27	,	,	PUNCT
eurjchem-2064	130	28	j	j	PROPN
eurjchem-2064	130	29	=	=	SYM
eurjchem-2064	130	30	8.1	8.1	NUM
eurjchem-2064	130	31	hz	hz	NOUN
eurjchem-2064	130	32	,	,	PUNCT
eurjchem-2064	130	33	2h	2h	NUM
eurjchem-2064	130	34	)	)	PUNCT
eurjchem-2064	130	35	,	,	PUNCT
eurjchem-2064	130	36	2.39	2.39	NUM
eurjchem-2064	130	37	(	(	PUNCT
eurjchem-2064	130	38	s	s	PROPN
eurjchem-2064	130	39	,	,	PUNCT
eurjchem-2064	130	40	3h	3h	NUM
eurjchem-2064	130	41	)	)	PUNCT
eurjchem-2064	130	42	,	,	PUNCT
eurjchem-2064	130	43	1.51	1.51	NUM
eurjchem-2064	130	44	(	(	PUNCT
eurjchem-2064	130	45	s	s	PROPN
eurjchem-2064	130	46	,	,	PUNCT
eurjchem-2064	130	47	2h	2h	NUM
eurjchem-2064	130	48	)	)	PUNCT
eurjchem-2064	130	49	,	,	PUNCT
eurjchem-2064	130	50	1.22	1.22	NUM
eurjchem-2064	130	51	(	(	PUNCT
eurjchem-2064	130	52	s	s	PROPN
eurjchem-2064	130	53	,	,	PUNCT
eurjchem-2064	130	54	6h	6h	NUM
eurjchem-2064	130	55	)	)	PUNCT
eurjchem-2064	130	56	,	,	PUNCT
eurjchem-2064	130	57	0.96	0.96	NUM
eurjchem-2064	130	58	(	(	PUNCT
eurjchem-2064	130	59	s	s	PROPN
eurjchem-2064	130	60	,	,	PUNCT
eurjchem-2064	130	61	9h	9h	NUM
eurjchem-2064	130	62	)	)	PUNCT
eurjchem-2064	130	63	.	.	PUNCT
eurjchem-2064	131	1	13c	13c	NOUN
eurjchem-2064	131	2	nmr	nmr	NOUN
eurjchem-2064	131	3	(	(	PUNCT
eurjchem-2064	131	4	100	100	NUM
eurjchem-2064	131	5	mhz	mhz	NOUN
eurjchem-2064	131	6	,	,	PUNCT
eurjchem-2064	131	7	chloroform	chloroform	NOUN
eurjchem-2064	131	8	-	-	PUNCT
eurjchem-2064	131	9	d	d	PROPN
eurjchem-2064	131	10	,	,	PUNCT
eurjchem-2064	131	11	δ	δ	PROPN
eurjchem-2064	131	12	,	,	PUNCT
eurjchem-2064	131	13	ppm	ppm	NUM
eurjchem-2064	131	14	):	):	PUNCT
eurjchem-2064	131	15	142.82	142.82	NUM
eurjchem-2064	131	16	,	,	PUNCT
eurjchem-2064	131	17	140.90	140.90	NUM
eurjchem-2064	131	18	,	,	PUNCT
eurjchem-2064	131	19	129.51	129.51	NUM
eurjchem-2064	131	20	,	,	PUNCT
eurjchem-2064	131	21	127.12	127.12	NUM
eurjchem-2064	131	22	,	,	PUNCT
eurjchem-2064	131	23	58.57	58.57	NUM
eurjchem-2064	131	24	,	,	PUNCT
eurjchem-2064	131	25	55.66	55.66	NUM
eurjchem-2064	131	26	,	,	PUNCT
eurjchem-2064	131	27	31.70	31.70	NUM
eurjchem-2064	131	28	,	,	PUNCT
eurjchem-2064	131	29	29.45	29.45	NUM
eurjchem-2064	131	30	,	,	PUNCT
eurjchem-2064	131	31	21.59	21.59	NUM
eurjchem-2064	131	32	.	.	NOUN
eurjchem-2064	131	33	4	4	NUM
eurjchem-2064	131	34	-	-	PUNCT
eurjchem-2064	131	35	methyl	methyl	NOUN
eurjchem-2064	131	36	-	-	PUNCT
eurjchem-2064	131	37	n-(1	n-(1	NOUN
eurjchem-2064	131	38	-	-	PUNCT
eurjchem-2064	131	39	phenylethyl)benzenesulfonamide	phenylethyl)benzenesulfonamide	ADJ
eurjchem-2064	131	40	(	(	PUNCT
eurjchem-2064	131	41	13	13	NUM
eurjchem-2064	131	42	):	):	PUNCT
eurjchem-2064	131	43	red	red	ADJ
eurjchem-2064	131	44	,	,	PUNCT
eurjchem-2064	131	45	slightly	slightly	ADV
eurjchem-2064	131	46	transparent	transparent	ADJ
eurjchem-2064	131	47	crystals	crystal	NOUN
eurjchem-2064	131	48	.	.	PUNCT
eurjchem-2064	132	1	m.p	m.p	PROPN
eurjchem-2064	132	2	.	.	PROPN
eurjchem-2064	132	3	:	:	PUNCT
eurjchem-2064	132	4	85	85	NUM
eurjchem-2064	132	5	-	-	SYM
eurjchem-2064	132	6	90	90	NUM
eurjchem-2064	132	7	°	°	NUM
eurjchem-2064	132	8	c	c	NOUN
eurjchem-2064	132	9	.	.	PUNCT
eurjchem-2064	133	1	rf	rf	NOUN
eurjchem-2064	133	2	=	=	NOUN
eurjchem-2064	133	3	0.54	0.54	NUM
eurjchem-2064	133	4	(	(	PUNCT
eurjchem-2064	133	5	ch2cl2	ch2cl2	NOUN
eurjchem-2064	133	6	)	)	PUNCT
eurjchem-2064	133	7	.	.	PUNCT
eurjchem-2064	134	1	1h	1h	NUM
eurjchem-2064	134	2	nmr	nmr	NOUN
eurjchem-2064	134	3	(	(	PUNCT
eurjchem-2064	134	4	400	400	NUM
eurjchem-2064	134	5	mhz	mhz	NOUN
eurjchem-2064	134	6	,	,	PUNCT
eurjchem-2064	134	7	chloroform	chloroform	NOUN
eurjchem-2064	134	8	-	-	PUNCT
eurjchem-2064	134	9	d	d	PROPN
eurjchem-2064	134	10	,	,	PUNCT
eurjchem-2064	134	11	δ	δ	PROPN
eurjchem-2064	134	12	,	,	PUNCT
eurjchem-2064	134	13	ppm	ppm	NOUN
eurjchem-2064	134	14	):	):	PUNCT
eurjchem-2064	134	15	7.64	7.64	NUM
eurjchem-2064	134	16	-	-	SYM
eurjchem-2064	134	17	7.58	7.58	NUM
eurjchem-2064	134	18	(	(	PUNCT
eurjchem-2064	134	19	m	m	PROPN
eurjchem-2064	134	20	,	,	PUNCT
eurjchem-2064	134	21	2h	2h	NUM
eurjchem-2064	134	22	)	)	PUNCT
eurjchem-2064	134	23	,	,	PUNCT
eurjchem-2064	134	24	7.18	7.18	NUM
eurjchem-2064	134	25	(	(	PUNCT
eurjchem-2064	134	26	qt	qt	PROPN
eurjchem-2064	134	27	,	,	PUNCT
eurjchem-2064	134	28	j	j	PROPN
eurjchem-2064	134	29	=	=	SYM
eurjchem-2064	134	30	4.3	4.3	NUM
eurjchem-2064	134	31	,	,	PUNCT
eurjchem-2064	134	32	2.6	2.6	NUM
eurjchem-2064	134	33	hz	hz	NOUN
eurjchem-2064	134	34	,	,	PUNCT
eurjchem-2064	134	35	5h	5h	NUM
eurjchem-2064	134	36	)	)	PUNCT
eurjchem-2064	134	37	,	,	PUNCT
eurjchem-2064	134	38	7.13	7.13	NUM
eurjchem-2064	134	39	-	-	SYM
eurjchem-2064	134	40	7.05	7.05	NUM
eurjchem-2064	134	41	(	(	PUNCT
eurjchem-2064	134	42	m	m	PROPN
eurjchem-2064	134	43	,	,	PUNCT
eurjchem-2064	134	44	2h	2h	NUM
eurjchem-2064	134	45	)	)	PUNCT
eurjchem-2064	134	46	,	,	PUNCT
eurjchem-2064	134	47	4.66	4.66	NUM
eurjchem-2064	134	48	(	(	PUNCT
eurjchem-2064	134	49	s	s	PROPN
eurjchem-2064	134	50	,	,	PUNCT
eurjchem-2064	134	51	1h	1h	NUM
eurjchem-2064	134	52	)	)	PUNCT
eurjchem-2064	134	53	,	,	PUNCT
eurjchem-2064	134	54	4.44	4.44	NUM
eurjchem-2064	134	55	(	(	PUNCT
eurjchem-2064	134	56	d	d	PROPN
eurjchem-2064	134	57	,	,	PUNCT
eurjchem-2064	134	58	j	j	PROPN
eurjchem-2064	134	59	=	=	SYM
eurjchem-2064	134	60	6.4	6.4	NUM
eurjchem-2064	134	61	hz	hz	NOUN
eurjchem-2064	134	62	,	,	PUNCT
eurjchem-2064	134	63	1h	1h	NUM
eurjchem-2064	134	64	)	)	PUNCT
eurjchem-2064	134	65	,	,	PUNCT
eurjchem-2064	134	66	2.38	2.38	NUM
eurjchem-2064	134	67	(	(	PUNCT
eurjchem-2064	134	68	s	s	PROPN
eurjchem-2064	134	69	,	,	PUNCT
eurjchem-2064	134	70	3h	3h	NUM
eurjchem-2064	134	71	)	)	PUNCT
eurjchem-2064	134	72	,	,	PUNCT
eurjchem-2064	134	73	1.41	1.41	NUM
eurjchem-2064	134	74	(	(	PUNCT
eurjchem-2064	134	75	dd	dd	PROPN
eurjchem-2064	134	76	,	,	PUNCT
eurjchem-2064	134	77	j	j	PROPN
eurjchem-2064	134	78	=	=	SYM
eurjchem-2064	134	79	7.4	7.4	NUM
eurjchem-2064	134	80	,	,	PUNCT
eurjchem-2064	134	81	2.9	2.9	NUM
eurjchem-2064	134	82	hz	hz	NOUN
eurjchem-2064	134	83	,	,	PUNCT
eurjchem-2064	134	84	3h	3h	NUM
eurjchem-2064	134	85	)	)	PUNCT
eurjchem-2064	134	86	.	.	PUNCT
eurjchem-2064	135	1	13c	13c	NOUN
eurjchem-2064	135	2	nmr	nmr	NOUN
eurjchem-2064	135	3	(	(	PUNCT
eurjchem-2064	135	4	100	100	NUM
eurjchem-2064	135	5	mhz	mhz	NOUN
eurjchem-2064	135	6	,	,	PUNCT
eurjchem-2064	135	7	chloroform	chloroform	NOUN
eurjchem-2064	135	8	-	-	PUNCT
eurjchem-2064	135	9	d	d	PROPN
eurjchem-2064	135	10	,	,	PUNCT
eurjchem-2064	135	11	δ	δ	PROPN
eurjchem-2064	135	12	,	,	PUNCT
eurjchem-2064	135	13	ppm	ppm	NOUN
eurjchem-2064	135	14	):	):	PUNCT
eurjchem-2064	135	15	143.18	143.18	NUM
eurjchem-2064	135	16	,	,	PUNCT
eurjchem-2064	135	17	142.23	142.23	NUM
eurjchem-2064	135	18	,	,	PUNCT
eurjchem-2064	135	19	137.71	137.71	NUM
eurjchem-2064	135	20	,	,	PUNCT
eurjchem-2064	135	21	129.53	129.53	NUM
eurjchem-2064	135	22	,	,	PUNCT
eurjchem-2064	135	23	128.58	128.58	NUM
eurjchem-2064	135	24	,	,	PUNCT
eurjchem-2064	135	25	127.46	127.46	NUM
eurjchem-2064	135	26	,	,	PUNCT
eurjchem-2064	135	27	127.19	127.19	NUM
eurjchem-2064	135	28	,	,	PUNCT
eurjchem-2064	135	29	126.24	126.24	NUM
eurjchem-2064	135	30	,	,	PUNCT
eurjchem-2064	135	31	53.75	53.75	NUM
eurjchem-2064	135	32	,	,	PUNCT
eurjchem-2064	135	33	23.68	23.68	NUM
eurjchem-2064	135	34	,	,	PUNCT
eurjchem-2064	135	35	21.59	21.59	NUM
eurjchem-2064	135	36	.	.	PUNCT
eurjchem-2064	136	1	stenfors	stenfor	NOUN
eurjchem-2064	136	2	and	and	CCONJ
eurjchem-2064	136	3	ngassa	ngassa	NOUN
eurjchem-2064	136	4	/	/	SYM
eurjchem-2064	136	5	european	european	ADJ
eurjchem-2064	136	6	journal	journal	PROPN
eurjchem-2064	136	7	of	of	ADP
eurjchem-2064	136	8	chemistry	chemistry	NOUN
eurjchem-2064	136	9	12	12	NUM
eurjchem-2064	136	10	(	(	PUNCT
eurjchem-2064	136	11	2	2	NUM
eurjchem-2064	136	12	)	)	PUNCT
eurjchem-2064	136	13	(	(	PUNCT
eurjchem-2064	136	14	2021	2021	NUM
eurjchem-2064	136	15	)	)	PUNCT
eurjchem-2064	136	16	109	109	NUM
eurjchem-2064	136	17	-	-	SYM
eurjchem-2064	136	18	116	116	NUM
eurjchem-2064	136	19	111	111	NUM
eurjchem-2064	136	20	2021	2021	NUM
eurjchem-2064	136	21	–	–	PUNCT
eurjchem-2064	136	22	european	european	ADJ
eurjchem-2064	136	23	journal	journal	NOUN
eurjchem-2064	136	24	of	of	ADP
eurjchem-2064	136	25	chemistry	chemistry	NOUN
eurjchem-2064	136	26	–	–	PUNCT
eurjchem-2064	136	27	cc	cc	NOUN
eurjchem-2064	136	28	by	by	ADP
eurjchem-2064	136	29	nc	nc	PROPN
eurjchem-2064	136	30	–	–	PUNCT
eurjchem-2064	136	31	doi	doi	NOUN
eurjchem-2064	136	32	:	:	PUNCT
eurjchem-2064	136	33	10.5155	10.5155	NUM
eurjchem-2064	136	34	/	/	SYM
eurjchem-2064	136	35	eurjchem.12.2.109	eurjchem.12.2.109	NUM
eurjchem-2064	136	36	-	-	PUNCT
eurjchem-2064	136	37	116.2064	116.2064	NUM
eurjchem-2064	136	38	figure	figure	NOUN
eurjchem-2064	136	39	2	2	NUM
eurjchem-2064	136	40	.	.	NOUN
eurjchem-2064	136	41	compounds	compound	VERB
eurjchem-2064	136	42	1	1	NUM
eurjchem-2064	136	43	-	-	SYM
eurjchem-2064	136	44	10	10	NUM
eurjchem-2064	136	45	,	,	PUNCT
eurjchem-2064	136	46	synthesized	synthesize	VERB
eurjchem-2064	136	47	by	by	ADP
eurjchem-2064	136	48	the	the	DET
eurjchem-2064	136	49	reaction	reaction	NOUN
eurjchem-2064	136	50	of	of	ADP
eurjchem-2064	136	51	4	4	NUM
eurjchem-2064	136	52	-	-	PUNCT
eurjchem-2064	136	53	methylbenzenesulfonyl	methylbenzenesulfonyl	NOUN
eurjchem-2064	136	54	chloride	chloride	NOUN
eurjchem-2064	136	55	and	and	CCONJ
eurjchem-2064	136	56	an	an	DET
eurjchem-2064	136	57	amine	amine	NOUN
eurjchem-2064	136	58	,	,	PUNCT
eurjchem-2064	136	59	in	in	ADP
eurjchem-2064	136	60	the	the	DET
eurjchem-2064	136	61	presence	presence	NOUN
eurjchem-2064	136	62	of	of	ADP
eurjchem-2064	136	63	pyridine	pyridine	NOUN
eurjchem-2064	136	64	and	and	CCONJ
eurjchem-2064	136	65	dichloromethane	dichloromethane	NOUN
eurjchem-2064	136	66	.	.	PUNCT
eurjchem-2064	137	1	reaction	reaction	NOUN
eurjchem-2064	137	2	conditions	condition	NOUN
eurjchem-2064	137	3	:	:	PUNCT
eurjchem-2064	137	4	4	4	NUM
eurjchem-2064	137	5	-	-	PUNCT
eurjchem-2064	137	6	methylbenzenesulfonyl	methylbenzenesulfonyl	NOUN
eurjchem-2064	137	7	chloride	chloride	NOUN
eurjchem-2064	137	8	(	(	PUNCT
eurjchem-2064	137	9	5.25	5.25	NUM
eurjchem-2064	137	10	mmol	mmol	NOUN
eurjchem-2064	137	11	,	,	PUNCT
eurjchem-2064	137	12	1.0	1.0	NUM
eurjchem-2064	137	13	eq	eq	NOUN
eurjchem-2064	137	14	)	)	PUNCT
eurjchem-2064	137	15	was	be	AUX
eurjchem-2064	137	16	dissolved	dissolve	VERB
eurjchem-2064	137	17	in	in	ADP
eurjchem-2064	137	18	10	10	NUM
eurjchem-2064	137	19	ml	ml	NOUN
eurjchem-2064	137	20	of	of	ADP
eurjchem-2064	137	21	dichloromethane	dichloromethane	NOUN
eurjchem-2064	137	22	,	,	PUNCT
eurjchem-2064	137	23	followed	follow	VERB
eurjchem-2064	137	24	by	by	ADP
eurjchem-2064	137	25	the	the	DET
eurjchem-2064	137	26	dropwise	dropwise	NOUN
eurjchem-2064	137	27	addition	addition	NOUN
eurjchem-2064	137	28	of	of	ADP
eurjchem-2064	137	29	the	the	DET
eurjchem-2064	137	30	amine	amine	ADJ
eurjchem-2064	137	31	(	(	PUNCT
eurjchem-2064	137	32	5.90	5.90	NUM
eurjchem-2064	137	33	mmol	mmol	NOUN
eurjchem-2064	137	34	,	,	PUNCT
eurjchem-2064	137	35	1.125	1.125	NUM
eurjchem-2064	137	36	eq	eq	NOUN
eurjchem-2064	137	37	)	)	PUNCT
eurjchem-2064	137	38	and	and	CCONJ
eurjchem-2064	137	39	pyridine	pyridine	NOUN
eurjchem-2064	137	40	(	(	PUNCT
eurjchem-2064	137	41	5.90	5.90	NUM
eurjchem-2064	137	42	mmol	mmol	NOUN
eurjchem-2064	137	43	,	,	PUNCT
eurjchem-2064	137	44	1.125	1.125	NUM
eurjchem-2064	137	45	eq	eq	NOUN
eurjchem-2064	137	46	)	)	PUNCT
eurjchem-2064	137	47	.	.	PUNCT
eurjchem-2064	138	1	reactions	reaction	NOUN
eurjchem-2064	138	2	were	be	AUX
eurjchem-2064	138	3	run	run	VERB
eurjchem-2064	138	4	at	at	ADP
eurjchem-2064	138	5	room	room	NOUN
eurjchem-2064	138	6	temperature	temperature	NOUN
eurjchem-2064	138	7	for	for	ADP
eurjchem-2064	138	8	24	24	NUM
eurjchem-2064	138	9	hours	hour	NOUN
eurjchem-2064	138	10	,	,	PUNCT
eurjchem-2064	138	11	under	under	ADP
eurjchem-2064	138	12	a	a	DET
eurjchem-2064	138	13	nitrogen	nitrogen	NOUN
eurjchem-2064	138	14	atmosphere	atmosphere	NOUN
eurjchem-2064	138	15	.	.	PUNCT
eurjchem-2064	139	1	2.1.3	2.1.3	X
eurjchem-2064	139	2	.	.	PUNCT
eurjchem-2064	139	3	general	general	ADJ
eurjchem-2064	139	4	procedure	procedure	NOUN
eurjchem-2064	139	5	for	for	ADP
eurjchem-2064	139	6	the	the	DET
eurjchem-2064	139	7	preparation	preparation	NOUN
eurjchem-2064	139	8	of	of	ADP
eurjchem-2064	139	9	sulfonamides	sulfonamide	NOUN
eurjchem-2064	139	10	synthesized	synthesize	VERB
eurjchem-2064	139	11	in	in	ADP
eurjchem-2064	139	12	the	the	DET
eurjchem-2064	139	13	presence	presence	NOUN
eurjchem-2064	139	14	of	of	ADP
eurjchem-2064	139	15	sodium	sodium	NOUN
eurjchem-2064	139	16	hydroxide	hydroxide	NOUN
eurjchem-2064	139	17	(	(	PUNCT
eurjchem-2064	139	18	2	2	NUM
eurjchem-2064	139	19	-	-	SYM
eurjchem-2064	139	20	4	4	NUM
eurjchem-2064	139	21	,	,	PUNCT
eurjchem-2064	139	22	8	8	NUM
eurjchem-2064	139	23	-	-	SYM
eurjchem-2064	139	24	10	10	NUM
eurjchem-2064	139	25	)	)	PUNCT
eurjchem-2064	139	26	4	4	NUM
eurjchem-2064	139	27	-	-	PUNCT
eurjchem-2064	139	28	methylbenzenesulfonyl	methylbenzenesulfonyl	NOUN
eurjchem-2064	139	29	chloride	chloride	NOUN
eurjchem-2064	139	30	(	(	PUNCT
eurjchem-2064	139	31	1.00	1.00	NUM
eurjchem-2064	139	32	g	g	NOUN
eurjchem-2064	139	33	,	,	PUNCT
eurjchem-2064	139	34	5.25	5.25	NUM
eurjchem-2064	139	35	mmol	mmol	NOUN
eurjchem-2064	139	36	)	)	PUNCT
eurjchem-2064	139	37	was	be	AUX
eurjchem-2064	139	38	added	add	VERB
eurjchem-2064	139	39	to	to	ADP
eurjchem-2064	139	40	a	a	DET
eurjchem-2064	139	41	flask	flask	NOUN
eurjchem-2064	139	42	containing	contain	VERB
eurjchem-2064	139	43	10	10	NUM
eurjchem-2064	139	44	ml	ml	NOUN
eurjchem-2064	139	45	of	of	ADP
eurjchem-2064	139	46	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-2064	139	47	.	.	PUNCT
eurjchem-2064	140	1	an	an	DET
eurjchem-2064	140	2	amine	amine	ADJ
eurjchem-2064	140	3	(	(	PUNCT
eurjchem-2064	140	4	5.90	5.90	NUM
eurjchem-2064	140	5	mmol	mmol	NOUN
eurjchem-2064	140	6	)	)	PUNCT
eurjchem-2064	140	7	was	be	AUX
eurjchem-2064	140	8	added	add	VERB
eurjchem-2064	140	9	dropwise	dropwise	NOUN
eurjchem-2064	140	10	to	to	ADP
eurjchem-2064	140	11	the	the	DET
eurjchem-2064	140	12	stirring	stirring	ADJ
eurjchem-2064	140	13	solution	solution	NOUN
eurjchem-2064	140	14	,	,	PUNCT
eurjchem-2064	140	15	followed	follow	VERB
eurjchem-2064	140	16	by	by	ADP
eurjchem-2064	140	17	the	the	DET
eurjchem-2064	140	18	dropwise	dropwise	NOUN
eurjchem-2064	140	19	addition	addition	NOUN
eurjchem-2064	140	20	of	of	ADP
eurjchem-2064	140	21	0.59	0.59	NUM
eurjchem-2064	140	22	m	m	PROPN
eurjchem-2064	140	23	aqueous	aqueous	ADJ
eurjchem-2064	140	24	sodium	sodium	NOUN
eurjchem-2064	140	25	hydroxide	hydroxide	NOUN
eurjchem-2064	140	26	(	(	PUNCT
eurjchem-2064	140	27	10	10	NUM
eurjchem-2064	140	28	ml	ml	NOUN
eurjchem-2064	140	29	,	,	PUNCT
eurjchem-2064	140	30	5.90	5.90	NUM
eurjchem-2064	140	31	mmol	mmol	NOUN
eurjchem-2064	140	32	)	)	PUNCT
eurjchem-2064	140	33	.	.	PUNCT
eurjchem-2064	141	1	the	the	DET
eurjchem-2064	141	2	flask	flask	NOUN
eurjchem-2064	141	3	was	be	AUX
eurjchem-2064	141	4	sealed	seal	VERB
eurjchem-2064	141	5	and	and	CCONJ
eurjchem-2064	141	6	left	leave	VERB
eurjchem-2064	141	7	to	to	PART
eurjchem-2064	141	8	react	react	VERB
eurjchem-2064	141	9	to	to	ADP
eurjchem-2064	141	10	completion	completion	NOUN
eurjchem-2064	141	11	at	at	ADP
eurjchem-2064	141	12	room	room	NOUN
eurjchem-2064	141	13	temperature	temperature	NOUN
eurjchem-2064	141	14	.	.	PUNCT
eurjchem-2064	142	1	reaction	reaction	NOUN
eurjchem-2064	142	2	completion	completion	NOUN
eurjchem-2064	142	3	was	be	AUX
eurjchem-2064	142	4	verified	verify	VERB
eurjchem-2064	142	5	by	by	ADP
eurjchem-2064	142	6	tlc	tlc	NOUN
eurjchem-2064	142	7	analysis	analysis	NOUN
eurjchem-2064	142	8	.	.	PUNCT
eurjchem-2064	143	1	the	the	DET
eurjchem-2064	143	2	mixture	mixture	NOUN
eurjchem-2064	143	3	was	be	AUX
eurjchem-2064	143	4	then	then	ADV
eurjchem-2064	143	5	concentrated	concentrate	VERB
eurjchem-2064	143	6	to	to	ADP
eurjchem-2064	143	7	half	half	DET
eurjchem-2064	143	8	its	its	PRON
eurjchem-2064	143	9	volume	volume	NOUN
eurjchem-2064	143	10	,	,	PUNCT
eurjchem-2064	143	11	acidified	acidify	VERB
eurjchem-2064	143	12	with	with	ADP
eurjchem-2064	143	13	5	5	NUM
eurjchem-2064	143	14	m	m	NOUN
eurjchem-2064	143	15	hcl	hcl	NOUN
eurjchem-2064	143	16	,	,	PUNCT
eurjchem-2064	143	17	and	and	CCONJ
eurjchem-2064	143	18	chilled	chill	VERB
eurjchem-2064	143	19	.	.	PUNCT
eurjchem-2064	144	1	the	the	DET
eurjchem-2064	144	2	resulting	result	VERB
eurjchem-2064	144	3	precipitate	precipitate	NOUN
eurjchem-2064	144	4	is	be	AUX
eurjchem-2064	144	5	isolated	isolate	VERB
eurjchem-2064	144	6	via	via	ADP
eurjchem-2064	144	7	vacuum	vacuum	NOUN
eurjchem-2064	144	8	filtration	filtration	NOUN
eurjchem-2064	144	9	and	and	CCONJ
eurjchem-2064	144	10	recrystallized	recrystallize	VERB
eurjchem-2064	144	11	from	from	ADP
eurjchem-2064	144	12	ethanol	ethanol	NOUN
eurjchem-2064	144	13	to	to	PART
eurjchem-2064	144	14	afford	afford	VERB
eurjchem-2064	144	15	the	the	DET
eurjchem-2064	144	16	product	product	NOUN
eurjchem-2064	144	17	in	in	ADP
eurjchem-2064	144	18	good	good	ADJ
eurjchem-2064	144	19	purity	purity	NOUN
eurjchem-2064	144	20	and	and	CCONJ
eurjchem-2064	144	21	yield	yield	NOUN
eurjchem-2064	144	22	.	.	PUNCT
eurjchem-2064	145	1	2.2	2.2	NUM
eurjchem-2064	145	2	.	.	PUNCT
eurjchem-2064	145	3	crystallographic	crystallographic	ADJ
eurjchem-2064	145	4	characterization	characterization	NOUN
eurjchem-2064	145	5	the	the	DET
eurjchem-2064	145	6	software	software	NOUN
eurjchem-2064	145	7	used	use	VERB
eurjchem-2064	145	8	for	for	ADP
eurjchem-2064	145	9	data	datum	NOUN
eurjchem-2064	145	10	collection	collection	NOUN
eurjchem-2064	145	11	is	be	AUX
eurjchem-2064	145	12	as	as	SCONJ
eurjchem-2064	145	13	follows	follow	VERB
eurjchem-2064	145	14	:	:	PUNCT
eurjchem-2064	145	15	data	data	NOUN
eurjchem-2064	145	16	collection	collection	NOUN
eurjchem-2064	145	17	,	,	PUNCT
eurjchem-2064	145	18	apex2	apex2	PUNCT
eurjchem-2064	146	1	[	[	X
eurjchem-2064	146	2	16	16	NUM
eurjchem-2064	146	3	]	]	X
eurjchem-2064	146	4	;	;	PUNCT
eurjchem-2064	146	5	cell	cell	NOUN
eurjchem-2064	146	6	refinement	refinement	NOUN
eurjchem-2064	146	7	and	and	CCONJ
eurjchem-2064	146	8	data	datum	NOUN
eurjchem-2064	146	9	reduction	reduction	NOUN
eurjchem-2064	146	10	,	,	PUNCT
eurjchem-2064	146	11	saint	saint	PROPN
eurjchem-2064	147	1	[	[	X
eurjchem-2064	147	2	17	17	NUM
eurjchem-2064	147	3	]	]	PUNCT
eurjchem-2064	147	4	;	;	PUNCT
eurjchem-2064	147	5	program	program	NOUN
eurjchem-2064	147	6	used	use	VERB
eurjchem-2064	147	7	to	to	PART
eurjchem-2064	147	8	refine	refine	VERB
eurjchem-2064	147	9	structure	structure	NOUN
eurjchem-2064	147	10	,	,	PUNCT
eurjchem-2064	147	11	shelxl	shelxl	VERB
eurjchem-2064	147	12	[	[	X
eurjchem-2064	147	13	18	18	NUM
eurjchem-2064	147	14	]	]	X
eurjchem-2064	147	15	;	;	PUNCT
eurjchem-2064	147	16	program	program	NOUN
eurjchem-2064	147	17	used	use	VERB
eurjchem-2064	147	18	to	to	PART
eurjchem-2064	147	19	solve	solve	VERB
eurjchem-2064	147	20	the	the	DET
eurjchem-2064	147	21	structure	structure	NOUN
eurjchem-2064	147	22	,	,	PUNCT
eurjchem-2064	147	23	shelxs	shelx	VERB
eurjchem-2064	148	1	[	[	X
eurjchem-2064	148	2	19	19	NUM
eurjchem-2064	148	3	]	]	X
eurjchem-2064	148	4	;	;	PUNCT
eurjchem-2064	148	5	molecular	molecular	ADJ
eurjchem-2064	148	6	graphics	graphic	NOUN
eurjchem-2064	148	7	and	and	CCONJ
eurjchem-2064	148	8	publication	publication	NOUN
eurjchem-2064	148	9	material	material	NOUN
eurjchem-2064	148	10	,	,	PUNCT
eurjchem-2064	148	11	olex2	olex2	PROPN
eurjchem-2064	149	1	[	[	X
eurjchem-2064	149	2	20,21	20,21	NUM
eurjchem-2064	149	3	]	]	X
eurjchem-2064	149	4	;	;	PUNCT
eurjchem-2064	149	5	program	program	NOUN
eurjchem-2064	149	6	used	use	VERB
eurjchem-2064	149	7	to	to	PART
eurjchem-2064	149	8	generate	generate	VERB
eurjchem-2064	149	9	figures	figure	NOUN
eurjchem-2064	149	10	,	,	PUNCT
eurjchem-2064	149	11	mercury	mercury	NOUN
eurjchem-2064	150	1	[	[	X
eurjchem-2064	150	2	22	22	NUM
eurjchem-2064	150	3	-	-	SYM
eurjchem-2064	150	4	26	26	NUM
eurjchem-2064	150	5	]	]	PUNCT
eurjchem-2064	150	6	;	;	PUNCT
eurjchem-2064	150	7	absorbance	absorbance	NOUN
eurjchem-2064	150	8	correction	correction	NOUN
eurjchem-2064	150	9	,	,	PUNCT
eurjchem-2064	150	10	sadabs	sadab	VERB
eurjchem-2064	151	1	[	[	X
eurjchem-2064	151	2	27	27	NUM
eurjchem-2064	151	3	]	]	PUNCT
eurjchem-2064	151	4	.	.	PUNCT
eurjchem-2064	152	1	hydrogen	hydrogen	NOUN
eurjchem-2064	152	2	atoms	atom	NOUN
eurjchem-2064	152	3	were	be	AUX
eurjchem-2064	152	4	refined	refine	VERB
eurjchem-2064	152	5	as	as	ADP
eurjchem-2064	152	6	riding	ride	VERB
eurjchem-2064	152	7	:	:	PUNCT
eurjchem-2064	152	8	c	c	X
eurjchem-2064	152	9	-	-	PUNCT
eurjchem-2064	152	10	h	h	NOUN
eurjchem-2064	152	11	=	=	NOUN
eurjchem-2064	152	12	0.95	0.95	NUM
eurjchem-2064	152	13	-	-	SYM
eurjchem-2064	152	14	1.00	1.00	NUM
eurjchem-2064	152	15	å	å	NOUN
eurjchem-2064	152	16	with	with	ADP
eurjchem-2064	152	17	uiso(h	uiso(h	PROPN
eurjchem-2064	152	18	)	)	PUNCT
eurjchem-2064	152	19	=	=	SYM
eurjchem-2064	152	20	1.5ueq(c	1.5ueq(c	X
eurjchem-2064	152	21	)	)	PUNCT
eurjchem-2064	152	22	for	for	ADP
eurjchem-2064	152	23	methyl	methyl	NOUN
eurjchem-2064	152	24	groups	group	NOUN
eurjchem-2064	152	25	,	,	PUNCT
eurjchem-2064	152	26	and	and	CCONJ
eurjchem-2064	152	27	uiso(h	uiso(h	PROPN
eurjchem-2064	152	28	)	)	PUNCT
eurjchem-2064	152	29	=	=	SYM
eurjchem-2064	152	30	1.2ueq(c	1.2ueq(c	NUM
eurjchem-2064	152	31	)	)	PUNCT
eurjchem-2064	152	32	for	for	ADP
eurjchem-2064	152	33	methylene	methylene	ADJ
eurjchem-2064	152	34	groups	group	NOUN
eurjchem-2064	152	35	and	and	CCONJ
eurjchem-2064	152	36	aromatic	aromatic	ADJ
eurjchem-2064	152	37	hydrogen	hydrogen	NOUN
eurjchem-2064	152	38	atoms	atom	NOUN
eurjchem-2064	152	39	.	.	PUNCT
eurjchem-2064	153	1	hydrogen	hydrogen	NOUN
eurjchem-2064	153	2	atom	atom	NOUN
eurjchem-2064	153	3	parameters	parameter	NOUN
eurjchem-2064	153	4	were	be	AUX
eurjchem-2064	153	5	constrained	constrain	VERB
eurjchem-2064	153	6	.	.	PUNCT
eurjchem-2064	154	1	2.3	2.3	NUM
eurjchem-2064	154	2	.	.	PUNCT
eurjchem-2064	155	1	instrumentation	instrumentation	NOUN
eurjchem-2064	155	2	1h	1h	NUM
eurjchem-2064	155	3	nmr	nmr	NOUN
eurjchem-2064	155	4	(	(	PUNCT
eurjchem-2064	155	5	400	400	NUM
eurjchem-2064	155	6	mhz	mhz	NOUN
eurjchem-2064	155	7	)	)	PUNCT
eurjchem-2064	155	8	and	and	CCONJ
eurjchem-2064	155	9	13c	13c	NOUN
eurjchem-2064	155	10	nmr	nmr	NOUN
eurjchem-2064	155	11	(	(	PUNCT
eurjchem-2064	155	12	100	100	NUM
eurjchem-2064	155	13	mhz	mhz	NOUN
eurjchem-2064	155	14	)	)	PUNCT
eurjchem-2064	155	15	spectra	spectra	NOUN
eurjchem-2064	155	16	were	be	AUX
eurjchem-2064	155	17	recorded	record	VERB
eurjchem-2064	155	18	on	on	ADP
eurjchem-2064	155	19	a	a	DET
eurjchem-2064	155	20	jeol	jeol	ADJ
eurjchem-2064	155	21	ecz400	ecz400	NOUN
eurjchem-2064	155	22	spectrometer	spectrometer	NOUN
eurjchem-2064	155	23	using	use	VERB
eurjchem-2064	155	24	a	a	DET
eurjchem-2064	155	25	dmso	dmso	NOUN
eurjchem-2064	155	26	-	-	ADJ
eurjchem-2064	155	27	d6	d6	NOUN
eurjchem-2064	155	28	or	or	CCONJ
eurjchem-2064	155	29	chloroform	chloroform	NOUN
eurjchem-2064	155	30	-	-	PUNCT
eurjchem-2064	155	31	d	d	NOUN
eurjchem-2064	155	32	solvent	solvent	NOUN
eurjchem-2064	155	33	.	.	PUNCT
eurjchem-2064	156	1	chemical	chemical	ADJ
eurjchem-2064	156	2	shifts	shift	NOUN
eurjchem-2064	156	3	are	be	AUX
eurjchem-2064	156	4	reported	report	VERB
eurjchem-2064	156	5	in	in	ADP
eurjchem-2064	156	6	parts	part	NOUN
eurjchem-2064	156	7	per	per	ADP
eurjchem-2064	156	8	million	million	NUM
eurjchem-2064	156	9	(	(	PUNCT
eurjchem-2064	156	10	ppm	ppm	PROPN
eurjchem-2064	156	11	,	,	PUNCT
eurjchem-2064	156	12	δ	δ	NOUN
eurjchem-2064	156	13	)	)	PUNCT
eurjchem-2064	156	14	relative	relative	ADJ
eurjchem-2064	156	15	to	to	ADP
eurjchem-2064	156	16	the	the	DET
eurjchem-2064	156	17	residual	residual	ADJ
eurjchem-2064	156	18	solvent	solvent	NOUN
eurjchem-2064	156	19	peak	peak	NOUN
eurjchem-2064	156	20	,	,	PUNCT
eurjchem-2064	156	21	and	and	CCONJ
eurjchem-2064	156	22	coupling	couple	VERB
eurjchem-2064	156	23	constants	constant	NOUN
eurjchem-2064	156	24	(	(	PUNCT
eurjchem-2064	156	25	j	j	NOUN
eurjchem-2064	156	26	)	)	PUNCT
eurjchem-2064	156	27	are	be	AUX
eurjchem-2064	156	28	reported	report	VERB
eurjchem-2064	156	29	in	in	ADP
eurjchem-2064	156	30	hertz	hertz	NOUN
eurjchem-2064	156	31	(	(	PUNCT
eurjchem-2064	156	32	hz	hz	PROPN
eurjchem-2064	156	33	)	)	PUNCT
eurjchem-2064	156	34	.	.	PUNCT
eurjchem-2064	157	1	x	x	X
eurjchem-2064	157	2	-	-	PUNCT
eurjchem-2064	157	3	ray	ray	NOUN
eurjchem-2064	157	4	diffraction	diffraction	NOUN
eurjchem-2064	157	5	was	be	AUX
eurjchem-2064	157	6	carried	carry	VERB
eurjchem-2064	157	7	out	out	ADP
eurjchem-2064	157	8	on	on	ADP
eurjchem-2064	157	9	a	a	DET
eurjchem-2064	157	10	bruker	bruker	NOUN
eurjchem-2064	157	11	apexii	apexii	NOUN
eurjchem-2064	157	12	ccd	ccd	PROPN
eurjchem-2064	157	13	diffracttometer	diffracttometer	ADV
eurjchem-2064	157	14	with	with	ADP
eurjchem-2064	157	15	mokα	mokα	ADJ
eurjchem-2064	157	16	radiation	radiation	NOUN
eurjchem-2064	157	17	.	.	PUNCT
eurjchem-2064	158	1	3	3	X
eurjchem-2064	158	2	.	.	X
eurjchem-2064	158	3	results	result	NOUN
eurjchem-2064	158	4	and	and	CCONJ
eurjchem-2064	158	5	discussion	discussion	NOUN
eurjchem-2064	158	6	3.1	3.1	NUM
eurjchem-2064	158	7	.	.	PUNCT
eurjchem-2064	158	8	tosylation	tosylation	NOUN
eurjchem-2064	158	9	of	of	ADP
eurjchem-2064	158	10	amines	amine	NOUN
eurjchem-2064	158	11	preliminary	preliminary	ADJ
eurjchem-2064	158	12	experimentation	experimentation	NOUN
eurjchem-2064	158	13	involved	involve	VERB
eurjchem-2064	158	14	the	the	DET
eurjchem-2064	158	15	amination	amination	NOUN
eurjchem-2064	158	16	of	of	ADP
eurjchem-2064	158	17	4methylbenzenesulfonyl	4methylbenzenesulfonyl	NUM
eurjchem-2064	158	18	chloride	chloride	NOUN
eurjchem-2064	158	19	or	or	CCONJ
eurjchem-2064	158	20	tosyl	tosyl	ADJ
eurjchem-2064	158	21	chloride	chloride	NOUN
eurjchem-2064	158	22	in	in	ADP
eurjchem-2064	158	23	the	the	DET
eurjchem-2064	158	24	presence	presence	NOUN
eurjchem-2064	158	25	of	of	ADP
eurjchem-2064	158	26	dichloromethane	dichloromethane	NOUN
eurjchem-2064	158	27	and	and	CCONJ
eurjchem-2064	158	28	pyridine	pyridine	NOUN
eurjchem-2064	158	29	.	.	PUNCT
eurjchem-2064	159	1	a	a	DET
eurjchem-2064	159	2	variety	variety	NOUN
eurjchem-2064	159	3	of	of	ADP
eurjchem-2064	159	4	primary	primary	ADJ
eurjchem-2064	159	5	,	,	PUNCT
eurjchem-2064	159	6	secondary	secondary	ADJ
eurjchem-2064	159	7	,	,	PUNCT
eurjchem-2064	159	8	and	and	CCONJ
eurjchem-2064	159	9	heterocyclic	heterocyclic	ADJ
eurjchem-2064	159	10	amines	amine	NOUN
eurjchem-2064	159	11	were	be	AUX
eurjchem-2064	159	12	used	use	VERB
eurjchem-2064	159	13	in	in	ADP
eurjchem-2064	159	14	the	the	DET
eurjchem-2064	159	15	synthesis	synthesis	NOUN
eurjchem-2064	159	16	of	of	ADP
eurjchem-2064	159	17	sulfonamides	sulfonamide	NOUN
eurjchem-2064	159	18	.	.	PUNCT
eurjchem-2064	160	1	these	these	DET
eurjchem-2064	160	2	amines	amine	NOUN
eurjchem-2064	160	3	were	be	AUX
eurjchem-2064	160	4	selected	select	VERB
eurjchem-2064	160	5	based	base	VERB
eurjchem-2064	160	6	on	on	ADP
eurjchem-2064	160	7	their	their	PRON
eurjchem-2064	160	8	similarity	similarity	NOUN
eurjchem-2064	160	9	in	in	ADP
eurjchem-2064	160	10	structural	structural	ADJ
eurjchem-2064	160	11	features	feature	NOUN
eurjchem-2064	160	12	to	to	ADP
eurjchem-2064	160	13	existing	exist	VERB
eurjchem-2064	160	14	sulfonamide	sulfonamide	NOUN
eurjchem-2064	160	15	drugs	drug	NOUN
eurjchem-2064	160	16	.	.	PUNCT
eurjchem-2064	161	1	the	the	DET
eurjchem-2064	161	2	resulting	result	VERB
eurjchem-2064	161	3	products	product	NOUN
eurjchem-2064	161	4	and	and	CCONJ
eurjchem-2064	161	5	corresponding	correspond	VERB
eurjchem-2064	161	6	yields	yield	NOUN
eurjchem-2064	161	7	are	be	AUX
eurjchem-2064	161	8	summarized	summarize	VERB
eurjchem-2064	161	9	in	in	ADP
eurjchem-2064	161	10	figure	figure	NOUN
eurjchem-2064	161	11	2	2	NUM
eurjchem-2064	161	12	.	.	PUNCT
eurjchem-2064	162	1	optimization	optimization	NOUN
eurjchem-2064	162	2	of	of	ADP
eurjchem-2064	162	3	reaction	reaction	NOUN
eurjchem-2064	162	4	conditions	condition	NOUN
eurjchem-2064	162	5	led	lead	VERB
eurjchem-2064	162	6	to	to	ADP
eurjchem-2064	162	7	the	the	DET
eurjchem-2064	162	8	development	development	NOUN
eurjchem-2064	162	9	of	of	ADP
eurjchem-2064	162	10	a	a	DET
eurjchem-2064	162	11	miscible	miscible	ADJ
eurjchem-2064	162	12	biphasic	biphasic	ADJ
eurjchem-2064	162	13	solvent	solvent	NOUN
eurjchem-2064	162	14	system	system	NOUN
eurjchem-2064	162	15	amenable	amenable	ADJ
eurjchem-2064	162	16	to	to	ADP
eurjchem-2064	162	17	various	various	ADJ
eurjchem-2064	162	18	reagents	reagent	NOUN
eurjchem-2064	162	19	.	.	PUNCT
eurjchem-2064	163	1	these	these	DET
eurjchem-2064	163	2	changes	change	NOUN
eurjchem-2064	163	3	led	lead	VERB
eurjchem-2064	163	4	to	to	PART
eurjchem-2064	163	5	decreased	decrease	VERB
eurjchem-2064	163	6	reaction	reaction	NOUN
eurjchem-2064	163	7	times	time	NOUN
eurjchem-2064	163	8	,	,	PUNCT
eurjchem-2064	163	9	improved	improved	ADJ
eurjchem-2064	163	10	yields	yield	NOUN
eurjchem-2064	163	11	,	,	PUNCT
eurjchem-2064	163	12	and	and	CCONJ
eurjchem-2064	163	13	ease	ease	NOUN
eurjchem-2064	163	14	of	of	ADP
eurjchem-2064	163	15	workup	workup	NOUN
eurjchem-2064	163	16	.	.	PUNCT
eurjchem-2064	164	1	in	in	ADP
eurjchem-2064	164	2	most	most	ADJ
eurjchem-2064	164	3	cases	case	NOUN
eurjchem-2064	164	4	,	,	PUNCT
eurjchem-2064	164	5	high	high	ADJ
eurjchem-2064	164	6	purity	purity	NOUN
eurjchem-2064	164	7	products	product	NOUN
eurjchem-2064	164	8	could	could	AUX
eurjchem-2064	164	9	be	be	AUX
eurjchem-2064	164	10	isolated	isolate	VERB
eurjchem-2064	164	11	directly	directly	ADV
eurjchem-2064	164	12	from	from	ADP
eurjchem-2064	164	13	the	the	DET
eurjchem-2064	164	14	reaction	reaction	NOUN
eurjchem-2064	164	15	mixture	mixture	NOUN
eurjchem-2064	164	16	after	after	ADP
eurjchem-2064	164	17	acidification	acidification	NOUN
eurjchem-2064	164	18	without	without	ADP
eurjchem-2064	164	19	further	further	ADJ
eurjchem-2064	164	20	purification	purification	NOUN
eurjchem-2064	164	21	.	.	PUNCT
eurjchem-2064	165	1	a	a	DET
eurjchem-2064	165	2	variety	variety	NOUN
eurjchem-2064	165	3	of	of	ADP
eurjchem-2064	165	4	reagents	reagent	NOUN
eurjchem-2064	165	5	and	and	CCONJ
eurjchem-2064	165	6	solvent	solvent	NOUN
eurjchem-2064	165	7	combinations	combination	NOUN
eurjchem-2064	165	8	were	be	AUX
eurjchem-2064	165	9	implemented	implement	VERB
eurjchem-2064	165	10	in	in	ADP
eurjchem-2064	165	11	the	the	DET
eurjchem-2064	165	12	synthesis	synthesis	NOUN
eurjchem-2064	165	13	of	of	ADP
eurjchem-2064	165	14	1-[(4	1-[(4	ADV
eurjchem-2064	165	15	-	-	PUNCT
eurjchem-2064	165	16	methylbenzene)sulfonyl]pyrrolidine	methylbenzene)sulfonyl]pyrrolidine	NOUN
eurjchem-2064	165	17	(	(	PUNCT
eurjchem-2064	165	18	3	3	NUM
eurjchem-2064	165	19	;	;	PUNCT
eurjchem-2064	165	20	table	table	NOUN
eurjchem-2064	165	21	1	1	NUM
eurjchem-2064	165	22	)	)	PUNCT
eurjchem-2064	165	23	.	.	PUNCT
eurjchem-2064	166	1	entries	entry	NOUN
eurjchem-2064	166	2	5	5	NUM
eurjchem-2064	166	3	and	and	CCONJ
eurjchem-2064	166	4	6	6	NUM
eurjchem-2064	166	5	show	show	VERB
eurjchem-2064	166	6	the	the	DET
eurjchem-2064	166	7	effect	effect	NOUN
eurjchem-2064	166	8	of	of	ADP
eurjchem-2064	166	9	solvent	solvent	ADJ
eurjchem-2064	166	10	change	change	NOUN
eurjchem-2064	166	11	without	without	ADP
eurjchem-2064	166	12	the	the	DET
eurjchem-2064	166	13	presence	presence	NOUN
eurjchem-2064	166	14	of	of	ADP
eurjchem-2064	166	15	an	an	DET
eurjchem-2064	166	16	acid	acid	NOUN
eurjchem-2064	166	17	scavenger	scavenger	NOUN
eurjchem-2064	166	18	.	.	PUNCT
eurjchem-2064	167	1	a	a	DET
eurjchem-2064	167	2	comparison	comparison	NOUN
eurjchem-2064	167	3	of	of	ADP
eurjchem-2064	167	4	entries	entry	NOUN
eurjchem-2064	167	5	5	5	NUM
eurjchem-2064	167	6	and	and	CCONJ
eurjchem-2064	167	7	6	6	NUM
eurjchem-2064	167	8	lends	lend	VERB
eurjchem-2064	167	9	credence	credence	NOUN
eurjchem-2064	167	10	to	to	ADP
eurjchem-2064	167	11	conditions	condition	NOUN
eurjchem-2064	167	12	that	that	PRON
eurjchem-2064	167	13	favor	favor	VERB
eurjchem-2064	167	14	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-2064	167	15	over	over	ADP
eurjchem-2064	167	16	dichloromethane	dichloromethane	NOUN
eurjchem-2064	167	17	.	.	PUNCT
eurjchem-2064	168	1	a	a	DET
eurjchem-2064	168	2	comparison	comparison	NOUN
eurjchem-2064	168	3	of	of	ADP
eurjchem-2064	168	4	entries	entry	NOUN
eurjchem-2064	168	5	3	3	NUM
eurjchem-2064	168	6	and	and	CCONJ
eurjchem-2064	168	7	4	4	NUM
eurjchem-2064	168	8	,	,	PUNCT
eurjchem-2064	168	9	carried	carry	VERB
eurjchem-2064	168	10	out	out	ADP
eurjchem-2064	168	11	in	in	ADP
eurjchem-2064	168	12	the	the	DET
eurjchem-2064	168	13	presence	presence	NOUN
eurjchem-2064	168	14	of	of	ADP
eurjchem-2064	168	15	pyridine	pyridine	NOUN
eurjchem-2064	168	16	,	,	PUNCT
eurjchem-2064	168	17	lends	lend	VERB
eurjchem-2064	168	18	support	support	NOUN
eurjchem-2064	168	19	to	to	ADP
eurjchem-2064	168	20	the	the	DET
eurjchem-2064	168	21	same	same	ADJ
eurjchem-2064	168	22	conclusion	conclusion	NOUN
eurjchem-2064	168	23	.	.	PUNCT
eurjchem-2064	169	1	the	the	DET
eurjchem-2064	169	2	use	use	NOUN
eurjchem-2064	169	3	of	of	ADP
eurjchem-2064	169	4	potassium	potassium	NOUN
eurjchem-2064	169	5	carbonate	carbonate	NOUN
eurjchem-2064	169	6	and	and	CCONJ
eurjchem-2064	169	7	sodium	sodium	NOUN
eurjchem-2064	169	8	hydroxide	hydroxide	NOUN
eurjchem-2064	169	9	aqueous	aqueous	ADJ
eurjchem-2064	169	10	bases	basis	NOUN
eurjchem-2064	169	11	proved	prove	VERB
eurjchem-2064	169	12	advantageous	advantageous	ADJ
eurjchem-2064	169	13	over	over	ADP
eurjchem-2064	169	14	the	the	DET
eurjchem-2064	169	15	previous	previous	ADJ
eurjchem-2064	169	16	method	method	NOUN
eurjchem-2064	169	17	with	with	ADP
eurjchem-2064	169	18	yields	yield	NOUN
eurjchem-2064	169	19	of	of	ADP
eurjchem-2064	169	20	91	91	NUM
eurjchem-2064	169	21	%	%	NOUN
eurjchem-2064	169	22	.	.	PUNCT
eurjchem-2064	170	1	entry	entry	NOUN
eurjchem-2064	170	2	1	1	NUM
eurjchem-2064	170	3	resulted	result	VERB
eurjchem-2064	170	4	in	in	ADP
eurjchem-2064	170	5	a	a	DET
eurjchem-2064	170	6	reaction	reaction	NOUN
eurjchem-2064	170	7	time	time	NOUN
eurjchem-2064	170	8	of	of	ADP
eurjchem-2064	170	9	6	6	NUM
eurjchem-2064	170	10	hours	hour	NOUN
eurjchem-2064	170	11	using	use	VERB
eurjchem-2064	170	12	potassium	potassium	NOUN
eurjchem-2064	170	13	carbonate	carbonate	NOUN
eurjchem-2064	170	14	.	.	PUNCT
eurjchem-2064	171	1	the	the	DET
eurjchem-2064	171	2	use	use	NOUN
eurjchem-2064	171	3	of	of	ADP
eurjchem-2064	171	4	sodium	sodium	NOUN
eurjchem-2064	171	5	hydroxide	hydroxide	NOUN
eurjchem-2064	171	6	resulted	result	VERB
eurjchem-2064	171	7	in	in	ADP
eurjchem-2064	171	8	a	a	DET
eurjchem-2064	171	9	reaction	reaction	NOUN
eurjchem-2064	171	10	time	time	NOUN
eurjchem-2064	171	11	of	of	ADP
eurjchem-2064	171	12	only	only	ADV
eurjchem-2064	171	13	3	3	NUM
eurjchem-2064	171	14	hours	hour	NOUN
eurjchem-2064	171	15	for	for	ADP
eurjchem-2064	171	16	entry	entry	NOUN
eurjchem-2064	171	17	2	2	NUM
eurjchem-2064	171	18	,	,	PUNCT
eurjchem-2064	171	19	without	without	ADP
eurjchem-2064	171	20	sacrificing	sacrifice	VERB
eurjchem-2064	171	21	yield	yield	NOUN
eurjchem-2064	171	22	.	.	PUNCT
eurjchem-2064	172	1	this	this	DET
eurjchem-2064	172	2	occurrence	occurrence	NOUN
eurjchem-2064	172	3	may	may	AUX
eurjchem-2064	172	4	be	be	AUX
eurjchem-2064	172	5	due	due	ADJ
eurjchem-2064	172	6	to	to	ADP
eurjchem-2064	172	7	the	the	DET
eurjchem-2064	172	8	increased	increase	VERB
eurjchem-2064	172	9	basicity	basicity	NOUN
eurjchem-2064	172	10	of	of	ADP
eurjchem-2064	172	11	sodium	sodium	NOUN
eurjchem-2064	172	12	hydroxide	hydroxide	NOUN
eurjchem-2064	172	13	.	.	PUNCT
eurjchem-2064	173	1	methods	method	NOUN
eurjchem-2064	173	2	involving	involve	VERB
eurjchem-2064	173	3	the	the	DET
eurjchem-2064	173	4	use	use	NOUN
eurjchem-2064	173	5	of	of	ADP
eurjchem-2064	173	6	aqueous	aqueous	ADJ
eurjchem-2064	173	7	base	base	NOUN
eurjchem-2064	173	8	and	and	CCONJ
eurjchem-2064	173	9	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-2064	173	10	proved	prove	VERB
eurjchem-2064	173	11	most	most	ADV
eurjchem-2064	173	12	effective	effective	ADJ
eurjchem-2064	173	13	.	.	PUNCT
eurjchem-2064	174	1	furthermore	furthermore	ADV
eurjchem-2064	174	2	,	,	PUNCT
eurjchem-2064	174	3	the	the	DET
eurjchem-2064	174	4	use	use	NOUN
eurjchem-2064	174	5	of	of	ADP
eurjchem-2064	174	6	less	less	ADV
eurjchem-2064	174	7	toxic	toxic	ADJ
eurjchem-2064	174	8	solvents	solvent	NOUN
eurjchem-2064	174	9	and	and	CCONJ
eurjchem-2064	174	10	reagents	reagent	NOUN
eurjchem-2064	174	11	lends	lend	VERB
eurjchem-2064	174	12	credence	credence	NOUN
eurjchem-2064	174	13	to	to	ADP
eurjchem-2064	174	14	an	an	DET
eurjchem-2064	174	15	environmentally	environmentally	ADV
eurjchem-2064	174	16	benign	benign	ADJ
eurjchem-2064	174	17	synthesis	synthesis	NOUN
eurjchem-2064	174	18	of	of	ADP
eurjchem-2064	174	19	sulfonamides	sulfonamide	NOUN
eurjchem-2064	174	20	.	.	PUNCT
eurjchem-2064	175	1	reactions	reaction	NOUN
eurjchem-2064	175	2	involving	involve	VERB
eurjchem-2064	175	3	pyridine	pyridine	NOUN
eurjchem-2064	175	4	were	be	AUX
eurjchem-2064	175	5	conducted	conduct	VERB
eurjchem-2064	175	6	under	under	ADP
eurjchem-2064	175	7	an	an	DET
eurjchem-2064	175	8	inert	inert	ADJ
eurjchem-2064	175	9	atmosphere	atmosphere	NOUN
eurjchem-2064	175	10	due	due	ADP
eurjchem-2064	175	11	to	to	ADP
eurjchem-2064	175	12	concerns	concern	NOUN
eurjchem-2064	175	13	regarding	regard	VERB
eurjchem-2064	175	14	the	the	DET
eurjchem-2064	175	15	hydrolysis	hydrolysis	NOUN
eurjchem-2064	175	16	of	of	ADP
eurjchem-2064	175	17	the	the	DET
eurjchem-2064	175	18	n	n	CCONJ
eurjchem-2064	175	19	-	-	PUNCT
eurjchem-2064	175	20	tosylpyridinium	tosylpyridinium	NOUN
eurjchem-2064	175	21	salt	salt	NOUN
eurjchem-2064	175	22	intermediate	intermediate	ADJ
eurjchem-2064	175	23	.	.	PUNCT
eurjchem-2064	176	1	previously	previously	ADV
eurjchem-2064	176	2	reported	report	VERB
eurjchem-2064	176	3	work	work	NOUN
eurjchem-2064	176	4	provides	provide	VERB
eurjchem-2064	176	5	mechanistic	mechanistic	ADJ
eurjchem-2064	176	6	insight	insight	NOUN
eurjchem-2064	176	7	into	into	ADP
eurjchem-2064	176	8	the	the	DET
eurjchem-2064	176	9	formation	formation	NOUN
eurjchem-2064	176	10	of	of	ADP
eurjchem-2064	176	11	ntosylpyridinium	ntosylpyridinium	NOUN
eurjchem-2064	176	12	in	in	ADP
eurjchem-2064	176	13	the	the	DET
eurjchem-2064	176	14	context	context	NOUN
eurjchem-2064	176	15	of	of	ADP
eurjchem-2064	176	16	sulfonates	sulfonate	NOUN
eurjchem-2064	176	17	[	[	X
eurjchem-2064	176	18	28	28	NUM
eurjchem-2064	176	19	]	]	PUNCT
eurjchem-2064	176	20	.	.	PUNCT
eurjchem-2064	177	1	however	however	ADV
eurjchem-2064	177	2	,	,	PUNCT
eurjchem-2064	177	3	after	after	ADP
eurjchem-2064	177	4	achieving	achieve	VERB
eurjchem-2064	177	5	higher	high	ADJ
eurjchem-2064	177	6	yields	yield	NOUN
eurjchem-2064	177	7	in	in	ADP
eurjchem-2064	177	8	the	the	DET
eurjchem-2064	177	9	presence	presence	NOUN
eurjchem-2064	177	10	of	of	ADP
eurjchem-2064	177	11	aqueous	aqueous	ADJ
eurjchem-2064	177	12	pyridine	pyridine	NOUN
eurjchem-2064	177	13	and	and	CCONJ
eurjchem-2064	177	14	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-2064	177	15	it	it	PRON
eurjchem-2064	177	16	was	be	AUX
eurjchem-2064	177	17	concluded	conclude	VERB
eurjchem-2064	177	18	that	that	SCONJ
eurjchem-2064	177	19	the	the	DET
eurjchem-2064	177	20	rate	rate	NOUN
eurjchem-2064	177	21	of	of	ADP
eurjchem-2064	177	22	hydrolysis	hydrolysis	NOUN
eurjchem-2064	177	23	is	be	AUX
eurjchem-2064	177	24	insignificant	insignificant	ADJ
eurjchem-2064	177	25	compared	compare	VERB
eurjchem-2064	177	26	to	to	ADP
eurjchem-2064	177	27	the	the	DET
eurjchem-2064	177	28	solvent	solvent	ADJ
eurjchem-2064	177	29	and	and	CCONJ
eurjchem-2064	177	30	base	base	NOUN
eurjchem-2064	177	31	combination	combination	NOUN
eurjchem-2064	177	32	chosen	choose	VERB
eurjchem-2064	177	33	.	.	PUNCT
eurjchem-2064	178	1	having	have	VERB
eurjchem-2064	178	2	the	the	DET
eurjchem-2064	178	3	optimized	optimize	VERB
eurjchem-2064	178	4	conditions	condition	NOUN
eurjchem-2064	178	5	in	in	ADP
eurjchem-2064	178	6	hand	hand	NOUN
eurjchem-2064	178	7	,	,	PUNCT
eurjchem-2064	178	8	the	the	DET
eurjchem-2064	178	9	scope	scope	NOUN
eurjchem-2064	178	10	of	of	ADP
eurjchem-2064	178	11	the	the	DET
eurjchem-2064	178	12	reaction	reaction	NOUN
eurjchem-2064	178	13	of	of	ADP
eurjchem-2064	178	14	amines	amine	NOUN
eurjchem-2064	178	15	with	with	ADP
eurjchem-2064	178	16	4	4	NUM
eurjchem-2064	178	17	-	-	PUNCT
eurjchem-2064	178	18	methylbenzenesulfonyl	methylbenzenesulfonyl	ADJ
eurjchem-2064	178	19	chloride	chloride	NOUN
eurjchem-2064	178	20	was	be	AUX
eurjchem-2064	178	21	explored	explore	VERB
eurjchem-2064	178	22	,	,	PUNCT
eurjchem-2064	178	23	utilizing	utilize	VERB
eurjchem-2064	178	24	potassium	potassium	NOUN
eurjchem-2064	178	25	carbonate	carbonate	NOUN
eurjchem-2064	178	26	and	and	CCONJ
eurjchem-2064	178	27	sodium	sodium	NOUN
eurjchem-2064	178	28	hydroxide	hydroxide	NOUN
eurjchem-2064	178	29	(	(	PUNCT
eurjchem-2064	178	30	figure	figure	NOUN
eurjchem-2064	178	31	3	3	NUM
eurjchem-2064	178	32	)	)	PUNCT
eurjchem-2064	178	33	.	.	PUNCT
eurjchem-2064	179	1	yield	yield	NOUN
eurjchem-2064	179	2	increases	increase	NOUN
eurjchem-2064	179	3	are	be	AUX
eurjchem-2064	179	4	noted	note	VERB
eurjchem-2064	179	5	for	for	ADP
eurjchem-2064	179	6	either	either	CCONJ
eurjchem-2064	179	7	solvent	solvent	ADJ
eurjchem-2064	179	8	combination	combination	NOUN
eurjchem-2064	179	9	,	,	PUNCT
eurjchem-2064	179	10	though	though	SCONJ
eurjchem-2064	179	11	the	the	DET
eurjchem-2064	179	12	potassium	potassium	NOUN
eurjchem-2064	179	13	carbonate	carbonate	NOUN
eurjchem-2064	179	14	base	base	NOUN
eurjchem-2064	179	15	showed	show	VERB
eurjchem-2064	179	16	the	the	DET
eurjchem-2064	179	17	best	good	ADJ
eurjchem-2064	179	18	results	result	NOUN
eurjchem-2064	179	19	.	.	PUNCT
eurjchem-2064	180	1	reactions	reaction	NOUN
eurjchem-2064	180	2	in	in	ADP
eurjchem-2064	180	3	which	which	PRON
eurjchem-2064	180	4	sodium	sodium	NOUN
eurjchem-2064	180	5	hydroxide	hydroxide	NOUN
eurjchem-2064	180	6	was	be	AUX
eurjchem-2064	180	7	used	use	VERB
eurjchem-2064	180	8	exhibited	exhibit	VERB
eurjchem-2064	180	9	the	the	DET
eurjchem-2064	180	10	shortest	short	ADJ
eurjchem-2064	180	11	reaction	reaction	NOUN
eurjchem-2064	180	12	times	time	NOUN
eurjchem-2064	180	13	.	.	PUNCT
eurjchem-2064	181	1	112	112	NUM
eurjchem-2064	181	2	stenfors	stenfor	NOUN
eurjchem-2064	181	3	and	and	CCONJ
eurjchem-2064	181	4	ngassa	ngassa	NOUN
eurjchem-2064	181	5	/	/	SYM
eurjchem-2064	181	6	european	european	ADJ
eurjchem-2064	181	7	journal	journal	PROPN
eurjchem-2064	181	8	of	of	ADP
eurjchem-2064	181	9	chemistry	chemistry	NOUN
eurjchem-2064	181	10	12	12	NUM
eurjchem-2064	181	11	(	(	PUNCT
eurjchem-2064	181	12	2	2	NUM
eurjchem-2064	181	13	)	)	PUNCT
eurjchem-2064	181	14	(	(	PUNCT
eurjchem-2064	181	15	2021	2021	NUM
eurjchem-2064	181	16	)	)	PUNCT
eurjchem-2064	181	17	109	109	NUM
eurjchem-2064	181	18	-	-	SYM
eurjchem-2064	181	19	116	116	NUM
eurjchem-2064	181	20	2021	2021	NUM
eurjchem-2064	181	21	–	–	PUNCT
eurjchem-2064	181	22	european	european	ADJ
eurjchem-2064	181	23	journal	journal	NOUN
eurjchem-2064	181	24	of	of	ADP
eurjchem-2064	181	25	chemistry	chemistry	NOUN
eurjchem-2064	181	26	–	–	PUNCT
eurjchem-2064	181	27	cc	cc	NOUN
eurjchem-2064	181	28	by	by	ADP
eurjchem-2064	181	29	nc	nc	PROPN
eurjchem-2064	181	30	–	–	PUNCT
eurjchem-2064	181	31	doi	doi	NOUN
eurjchem-2064	181	32	:	:	PUNCT
eurjchem-2064	181	33	10.5155	10.5155	NUM
eurjchem-2064	181	34	/	/	SYM
eurjchem-2064	181	35	eurjchem.12.2.109	eurjchem.12.2.109	NUM
eurjchem-2064	181	36	-	-	PUNCT
eurjchem-2064	181	37	116.2064	116.2064	NUM
eurjchem-2064	181	38	table	table	NOUN
eurjchem-2064	181	39	1	1	NUM
eurjchem-2064	181	40	.	.	PUNCT
eurjchem-2064	181	41	base	base	NOUN
eurjchem-2064	181	42	and	and	CCONJ
eurjchem-2064	181	43	solvent	solvent	ADJ
eurjchem-2064	181	44	effects	effect	NOUN
eurjchem-2064	181	45	in	in	ADP
eurjchem-2064	181	46	the	the	DET
eurjchem-2064	181	47	synthesis	synthesis	NOUN
eurjchem-2064	181	48	of	of	ADP
eurjchem-2064	181	49	1-[(4	1-[(4	ADV
eurjchem-2064	181	50	-	-	PUNCT
eurjchem-2064	181	51	methylbenzene)sulfonyl]pyrrolidine	methylbenzene)sulfonyl]pyrrolidine	NOUN
eurjchem-2064	181	52	(	(	PUNCT
eurjchem-2064	181	53	3	3	NUM
eurjchem-2064	181	54	)	)	PUNCT
eurjchem-2064	181	55	,	,	PUNCT
eurjchem-2064	181	56	listed	list	VERB
eurjchem-2064	181	57	in	in	ADP
eurjchem-2064	181	58	order	order	NOUN
eurjchem-2064	181	59	of	of	ADP
eurjchem-2064	181	60	decreasing	decrease	VERB
eurjchem-2064	181	61	yield	yield	NOUN
eurjchem-2064	181	62	a.	a.	NOUN
eurjchem-2064	181	63	s	s	PART
eurjchem-2064	181	64	o	o	NOUN
eurjchem-2064	181	65	o	o	X
eurjchem-2064	181	66	cl	cl	NOUN
eurjchem-2064	182	1	+	+	CCONJ
eurjchem-2064	182	2	s	s	X
eurjchem-2064	182	3	o	o	X
eurjchem-2064	182	4	o	o	NOUN
eurjchem-2064	182	5	nnh	nnh	ADJ
eurjchem-2064	182	6	base	base	NOUN
eurjchem-2064	182	7	solvent	solvent	NOUN
eurjchem-2064	182	8	entry	entry	NOUN
eurjchem-2064	182	9	base	base	NOUN
eurjchem-2064	182	10	solvent	solvent	NOUN
eurjchem-2064	182	11	reaction	reaction	NOUN
eurjchem-2064	182	12	time	time	NOUN
eurjchem-2064	182	13	yield	yield	NOUN
eurjchem-2064	182	14	(	(	PUNCT
eurjchem-2064	182	15	%	%	NOUN
eurjchem-2064	182	16	)	)	PUNCT
eurjchem-2064	182	17	1	1	NUM
eurjchem-2064	182	18	0.59	0.59	NUM
eurjchem-2064	182	19	m	m	NOUN
eurjchem-2064	182	20	aq	aq	NOUN
eurjchem-2064	182	21	.	.	PUNCT
eurjchem-2064	182	22	k2co3	k2co3	ADJ
eurjchem-2064	182	23	thf	thf	NOUN
eurjchem-2064	182	24	6	6	NUM
eurjchem-2064	182	25	h	h	NOUN
eurjchem-2064	182	26	91	91	NUM
eurjchem-2064	182	27	2	2	NUM
eurjchem-2064	182	28	0.59	0.59	NUM
eurjchem-2064	182	29	m	m	NOUN
eurjchem-2064	182	30	aq	aq	NOUN
eurjchem-2064	182	31	.	.	PUNCT
eurjchem-2064	183	1	naoh	naoh	NOUN
eurjchem-2064	183	2	thf	thf	NOUN
eurjchem-2064	183	3	3	3	NUM
eurjchem-2064	183	4	h	h	NOUN
eurjchem-2064	183	5	91	91	NUM
eurjchem-2064	183	6	3	3	NUM
eurjchem-2064	183	7	0.59	0.59	NUM
eurjchem-2064	183	8	m	m	NOUN
eurjchem-2064	183	9	aq	aq	NOUN
eurjchem-2064	183	10	.	.	PUNCT
eurjchem-2064	183	11	pyridine	pyridine	NOUN
eurjchem-2064	183	12	thf	thf	NOUN
eurjchem-2064	183	13	24	24	NUM
eurjchem-2064	183	14	h	h	NOUN
eurjchem-2064	183	15	74	74	NUM
eurjchem-2064	183	16	4	4	NUM
eurjchem-2064	183	17	b	b	NOUN
eurjchem-2064	183	18	pyridine	pyridine	NOUN
eurjchem-2064	183	19	dcm	dcm	NOUN
eurjchem-2064	183	20	24	24	NUM
eurjchem-2064	183	21	h	h	NOUN
eurjchem-2064	183	22	57	57	NUM
eurjchem-2064	183	23	5	5	NUM
eurjchem-2064	183	24	thf	thf	NOUN
eurjchem-2064	183	25	24	24	NUM
eurjchem-2064	183	26	h	h	NOUN
eurjchem-2064	183	27	55	55	NUM
eurjchem-2064	183	28	6	6	NUM
eurjchem-2064	183	29	b	b	PROPN
eurjchem-2064	183	30	dcm	dcm	PROPN
eurjchem-2064	183	31	24	24	NUM
eurjchem-2064	183	32	h	h	NOUN
eurjchem-2064	183	33	26	26	NUM
eurjchem-2064	183	34	a	a	DET
eurjchem-2064	183	35	reaction	reaction	NOUN
eurjchem-2064	183	36	condition	condition	NOUN
eurjchem-2064	183	37	:	:	PUNCT
eurjchem-2064	183	38	4	4	NUM
eurjchem-2064	183	39	-	-	PUNCT
eurjchem-2064	183	40	methylbenzenesulfonyl	methylbenzenesulfonyl	NOUN
eurjchem-2064	183	41	chloride	chloride	NOUN
eurjchem-2064	183	42	(	(	PUNCT
eurjchem-2064	183	43	5.25	5.25	NUM
eurjchem-2064	183	44	mmol	mmol	NOUN
eurjchem-2064	183	45	,	,	PUNCT
eurjchem-2064	183	46	1.0	1.0	NUM
eurjchem-2064	183	47	eq	eq	NOUN
eurjchem-2064	183	48	.	.	PROPN
eurjchem-2064	183	49	)	)	PUNCT
eurjchem-2064	183	50	was	be	AUX
eurjchem-2064	183	51	dissolved	dissolve	VERB
eurjchem-2064	183	52	in	in	ADP
eurjchem-2064	183	53	10	10	NUM
eurjchem-2064	183	54	ml	ml	NOUN
eurjchem-2064	183	55	of	of	ADP
eurjchem-2064	183	56	solvent	solvent	NOUN
eurjchem-2064	183	57	,	,	PUNCT
eurjchem-2064	183	58	followed	follow	VERB
eurjchem-2064	183	59	by	by	ADP
eurjchem-2064	183	60	the	the	DET
eurjchem-2064	183	61	dropwise	dropwise	NOUN
eurjchem-2064	183	62	addition	addition	NOUN
eurjchem-2064	183	63	of	of	ADP
eurjchem-2064	183	64	both	both	DET
eurjchem-2064	183	65	pyrrolidine	pyrrolidine	NOUN
eurjchem-2064	183	66	(	(	PUNCT
eurjchem-2064	183	67	5.90	5.90	NUM
eurjchem-2064	183	68	mmol	mmol	NOUN
eurjchem-2064	183	69	,	,	PUNCT
eurjchem-2064	183	70	1.125	1.125	NUM
eurjchem-2064	183	71	eq	eq	NOUN
eurjchem-2064	183	72	.	.	PUNCT
eurjchem-2064	183	73	)	)	PUNCT
eurjchem-2064	184	1	and	and	CCONJ
eurjchem-2064	184	2	a	a	DET
eurjchem-2064	184	3	base	base	NOUN
eurjchem-2064	184	4	(	(	PUNCT
eurjchem-2064	184	5	5.90	5.90	NUM
eurjchem-2064	184	6	mmol	mmol	NOUN
eurjchem-2064	184	7	,	,	PUNCT
eurjchem-2064	184	8	1.125	1.125	NUM
eurjchem-2064	184	9	eq	eq	NOUN
eurjchem-2064	184	10	.	.	PUNCT
eurjchem-2064	184	11	)	)	PUNCT
eurjchem-2064	184	12	.	.	PUNCT
eurjchem-2064	185	1	reactions	reaction	NOUN
eurjchem-2064	185	2	were	be	AUX
eurjchem-2064	185	3	run	run	VERB
eurjchem-2064	185	4	at	at	ADP
eurjchem-2064	185	5	room	room	NOUN
eurjchem-2064	185	6	temperature	temperature	NOUN
eurjchem-2064	185	7	.	.	PUNCT
eurjchem-2064	186	1	b	b	X
eurjchem-2064	186	2	reaction	reaction	NOUN
eurjchem-2064	186	3	run	run	VERB
eurjchem-2064	186	4	under	under	ADP
eurjchem-2064	186	5	nitrogen	nitrogen	NOUN
eurjchem-2064	186	6	atmosphere	atmosphere	NOUN
eurjchem-2064	186	7	.	.	PUNCT
eurjchem-2064	187	1	figure	figure	VERB
eurjchem-2064	187	2	3	3	NUM
eurjchem-2064	187	3	.	.	NOUN
eurjchem-2064	187	4	compounds	compound	VERB
eurjchem-2064	187	5	1	1	NUM
eurjchem-2064	187	6	-	-	SYM
eurjchem-2064	187	7	13	13	NUM
eurjchem-2064	187	8	,	,	PUNCT
eurjchem-2064	187	9	synthesized	synthesize	VERB
eurjchem-2064	187	10	by	by	ADP
eurjchem-2064	187	11	the	the	DET
eurjchem-2064	187	12	reaction	reaction	NOUN
eurjchem-2064	187	13	of	of	ADP
eurjchem-2064	187	14	4	4	NUM
eurjchem-2064	187	15	-	-	PUNCT
eurjchem-2064	187	16	methylbenzenesulfonyl	methylbenzenesulfonyl	NOUN
eurjchem-2064	187	17	chloride	chloride	NOUN
eurjchem-2064	187	18	and	and	CCONJ
eurjchem-2064	187	19	an	an	DET
eurjchem-2064	187	20	amine	amine	NOUN
eurjchem-2064	187	21	,	,	PUNCT
eurjchem-2064	187	22	in	in	ADP
eurjchem-2064	187	23	the	the	DET
eurjchem-2064	187	24	presence	presence	NOUN
eurjchem-2064	187	25	of	of	ADP
eurjchem-2064	187	26	aqueous	aqueous	ADJ
eurjchem-2064	187	27	base	base	NOUN
eurjchem-2064	187	28	and	and	CCONJ
eurjchem-2064	187	29	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-2064	187	30	.	.	PUNCT
eurjchem-2064	188	1	reaction	reaction	NOUN
eurjchem-2064	188	2	conditions	condition	NOUN
eurjchem-2064	188	3	:	:	PUNCT
eurjchem-2064	188	4	4	4	NUM
eurjchem-2064	188	5	-	-	PUNCT
eurjchem-2064	188	6	methylbenzenesulfonyl	methylbenzenesulfonyl	NOUN
eurjchem-2064	188	7	chloride	chloride	NOUN
eurjchem-2064	188	8	(	(	PUNCT
eurjchem-2064	188	9	5.25	5.25	NUM
eurjchem-2064	188	10	mmol	mmol	NOUN
eurjchem-2064	188	11	,	,	PUNCT
eurjchem-2064	188	12	1.0	1.0	NUM
eurjchem-2064	188	13	eq	eq	NOUN
eurjchem-2064	188	14	)	)	PUNCT
eurjchem-2064	188	15	was	be	AUX
eurjchem-2064	188	16	dissolved	dissolve	VERB
eurjchem-2064	188	17	in	in	ADP
eurjchem-2064	188	18	10	10	NUM
eurjchem-2064	188	19	ml	ml	NOUN
eurjchem-2064	188	20	of	of	ADP
eurjchem-2064	188	21	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-2064	188	22	,	,	PUNCT
eurjchem-2064	188	23	followed	follow	VERB
eurjchem-2064	188	24	by	by	ADP
eurjchem-2064	188	25	the	the	DET
eurjchem-2064	188	26	dropwise	dropwise	NOUN
eurjchem-2064	188	27	addition	addition	NOUN
eurjchem-2064	188	28	of	of	ADP
eurjchem-2064	188	29	the	the	DET
eurjchem-2064	188	30	amine	amine	ADJ
eurjchem-2064	188	31	(	(	PUNCT
eurjchem-2064	188	32	5.90	5.90	NUM
eurjchem-2064	188	33	mmol	mmol	NOUN
eurjchem-2064	188	34	,	,	PUNCT
eurjchem-2064	188	35	1.125	1.125	NUM
eurjchem-2064	188	36	eq	eq	NOUN
eurjchem-2064	188	37	)	)	PUNCT
eurjchem-2064	188	38	and	and	CCONJ
eurjchem-2064	188	39	0.59	0.59	NUM
eurjchem-2064	188	40	m	m	NOUN
eurjchem-2064	188	41	aqueous	aqueous	ADJ
eurjchem-2064	188	42	base	base	NOUN
eurjchem-2064	188	43	(	(	PUNCT
eurjchem-2064	188	44	5.90	5.90	NUM
eurjchem-2064	188	45	mmol	mmol	NOUN
eurjchem-2064	188	46	,	,	PUNCT
eurjchem-2064	188	47	1.125	1.125	NUM
eurjchem-2064	188	48	eq	eq	NOUN
eurjchem-2064	188	49	)	)	PUNCT
eurjchem-2064	188	50	.	.	PUNCT
eurjchem-2064	189	1	reactions	reaction	NOUN
eurjchem-2064	189	2	were	be	AUX
eurjchem-2064	189	3	run	run	VERB
eurjchem-2064	189	4	at	at	ADP
eurjchem-2064	189	5	room	room	NOUN
eurjchem-2064	189	6	temperature	temperature	NOUN
eurjchem-2064	189	7	,	,	PUNCT
eurjchem-2064	189	8	reaction	reaction	NOUN
eurjchem-2064	189	9	completion	completion	NOUN
eurjchem-2064	189	10	verified	verify	VERB
eurjchem-2064	189	11	by	by	ADP
eurjchem-2064	189	12	tlc	tlc	PROPN
eurjchem-2064	189	13	.	.	PUNCT
eurjchem-2064	190	1	the	the	DET
eurjchem-2064	190	2	base	base	NOUN
eurjchem-2064	190	3	and	and	CCONJ
eurjchem-2064	190	4	solvent	solvent	ADJ
eurjchem-2064	190	5	effects	effect	NOUN
eurjchem-2064	190	6	were	be	AUX
eurjchem-2064	190	7	investigated	investigate	VERB
eurjchem-2064	190	8	in	in	ADP
eurjchem-2064	190	9	the	the	DET
eurjchem-2064	190	10	synthesis	synthesis	NOUN
eurjchem-2064	190	11	of	of	ADP
eurjchem-2064	190	12	n	n	X
eurjchem-2064	190	13	-	-	PUNCT
eurjchem-2064	190	14	butyl-4	butyl-4	NOUN
eurjchem-2064	190	15	-	-	PUNCT
eurjchem-2064	190	16	methylbenzenesulfonamide	methylbenzenesulfonamide	NOUN
eurjchem-2064	190	17	(	(	PUNCT
eurjchem-2064	190	18	4	4	NUM
eurjchem-2064	190	19	;	;	PUNCT
eurjchem-2064	190	20	table	table	NOUN
eurjchem-2064	190	21	2	2	NUM
eurjchem-2064	190	22	)	)	PUNCT
eurjchem-2064	190	23	.	.	PUNCT
eurjchem-2064	191	1	entry	entry	NOUN
eurjchem-2064	191	2	6	6	NUM
eurjchem-2064	191	3	in	in	ADP
eurjchem-2064	191	4	table	table	NOUN
eurjchem-2064	191	5	2	2	NUM
eurjchem-2064	191	6	represents	represent	VERB
eurjchem-2064	191	7	the	the	DET
eurjchem-2064	191	8	preliminary	preliminary	ADJ
eurjchem-2064	191	9	method	method	NOUN
eurjchem-2064	191	10	,	,	PUNCT
eurjchem-2064	191	11	with	with	ADP
eurjchem-2064	191	12	the	the	DET
eurjchem-2064	191	13	lowest	low	ADJ
eurjchem-2064	191	14	yield	yield	NOUN
eurjchem-2064	191	15	of	of	ADP
eurjchem-2064	191	16	54	54	NUM
eurjchem-2064	191	17	%	%	NOUN
eurjchem-2064	191	18	.	.	PUNCT
eurjchem-2064	192	1	entries	entry	NOUN
eurjchem-2064	192	2	1	1	NUM
eurjchem-2064	192	3	,	,	PUNCT
eurjchem-2064	192	4	2	2	NUM
eurjchem-2064	192	5	,	,	PUNCT
eurjchem-2064	192	6	and	and	CCONJ
eurjchem-2064	192	7	3	3	NUM
eurjchem-2064	192	8	in	in	ADP
eurjchem-2064	192	9	table	table	NOUN
eurjchem-2064	192	10	2	2	NUM
eurjchem-2064	192	11	with	with	ADP
eurjchem-2064	192	12	yields	yield	NOUN
eurjchem-2064	192	13	of	of	ADP
eurjchem-2064	192	14	90	90	NUM
eurjchem-2064	192	15	,	,	PUNCT
eurjchem-2064	192	16	82	82	NUM
eurjchem-2064	192	17	,	,	PUNCT
eurjchem-2064	192	18	and	and	CCONJ
eurjchem-2064	192	19	80	80	NUM
eurjchem-2064	192	20	%	%	NOUN
eurjchem-2064	192	21	,	,	PUNCT
eurjchem-2064	192	22	respectively	respectively	ADV
eurjchem-2064	192	23	,	,	PUNCT
eurjchem-2064	192	24	represent	represent	VERB
eurjchem-2064	192	25	the	the	DET
eurjchem-2064	192	26	effect	effect	NOUN
eurjchem-2064	192	27	of	of	ADP
eurjchem-2064	192	28	changing	change	VERB
eurjchem-2064	192	29	the	the	DET
eurjchem-2064	192	30	solvent	solvent	NOUN
eurjchem-2064	192	31	alone	alone	ADV
eurjchem-2064	192	32	.	.	PUNCT
eurjchem-2064	193	1	the	the	DET
eurjchem-2064	193	2	use	use	NOUN
eurjchem-2064	193	3	of	of	ADP
eurjchem-2064	193	4	acetone	acetone	NOUN
eurjchem-2064	193	5	and	and	CCONJ
eurjchem-2064	193	6	ethanol	ethanol	NOUN
eurjchem-2064	193	7	results	result	NOUN
eurjchem-2064	193	8	in	in	ADP
eurjchem-2064	193	9	lower	lower	ADV
eurjchem-2064	193	10	-	-	PUNCT
eurjchem-2064	193	11	yielding	yield	VERB
eurjchem-2064	193	12	reactions	reaction	NOUN
eurjchem-2064	193	13	than	than	ADP
eurjchem-2064	193	14	that	that	PRON
eurjchem-2064	193	15	of	of	ADP
eurjchem-2064	193	16	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-2064	193	17	.	.	PUNCT
eurjchem-2064	194	1	a	a	DET
eurjchem-2064	194	2	comparison	comparison	NOUN
eurjchem-2064	194	3	of	of	ADP
eurjchem-2064	194	4	entries	entry	NOUN
eurjchem-2064	194	5	1	1	NUM
eurjchem-2064	194	6	and	and	CCONJ
eurjchem-2064	194	7	4	4	NUM
eurjchem-2064	194	8	shows	show	VERB
eurjchem-2064	194	9	dramatic	dramatic	ADJ
eurjchem-2064	194	10	decreases	decrease	NOUN
eurjchem-2064	194	11	in	in	ADP
eurjchem-2064	194	12	yield	yield	NOUN
eurjchem-2064	194	13	from	from	ADP
eurjchem-2064	194	14	90	90	NUM
eurjchem-2064	194	15	to	to	PART
eurjchem-2064	194	16	77	77	NUM
eurjchem-2064	194	17	%	%	NOUN
eurjchem-2064	194	18	by	by	ADP
eurjchem-2064	194	19	doubling	double	VERB
eurjchem-2064	194	20	the	the	DET
eurjchem-2064	194	21	base	base	NOUN
eurjchem-2064	194	22	's	's	PART
eurjchem-2064	194	23	molarity	molarity	NOUN
eurjchem-2064	194	24	.	.	PUNCT
eurjchem-2064	195	1	it	it	PRON
eurjchem-2064	195	2	was	be	AUX
eurjchem-2064	195	3	concluded	conclude	VERB
eurjchem-2064	195	4	from	from	ADP
eurjchem-2064	195	5	the	the	DET
eurjchem-2064	195	6	results	result	NOUN
eurjchem-2064	195	7	that	that	PRON
eurjchem-2064	195	8	methods	method	NOUN
eurjchem-2064	195	9	involving	involve	VERB
eurjchem-2064	195	10	the	the	DET
eurjchem-2064	195	11	use	use	NOUN
eurjchem-2064	195	12	of	of	ADP
eurjchem-2064	195	13	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-2064	195	14	and	and	CCONJ
eurjchem-2064	195	15	0.59	0.59	NUM
eurjchem-2064	195	16	m	m	NOUN
eurjchem-2064	195	17	aqueous	aqueous	ADJ
eurjchem-2064	195	18	potassium	potassium	NOUN
eurjchem-2064	195	19	carbonate	carbonate	NOUN
eurjchem-2064	195	20	offered	offer	VERB
eurjchem-2064	195	21	the	the	DET
eurjchem-2064	195	22	best	good	ADJ
eurjchem-2064	195	23	combination	combination	NOUN
eurjchem-2064	195	24	of	of	ADP
eurjchem-2064	195	25	yield	yield	NOUN
eurjchem-2064	195	26	and	and	CCONJ
eurjchem-2064	195	27	reaction	reaction	NOUN
eurjchem-2064	195	28	time	time	NOUN
eurjchem-2064	195	29	while	while	SCONJ
eurjchem-2064	195	30	amenable	amenable	ADJ
eurjchem-2064	195	31	to	to	ADP
eurjchem-2064	195	32	a	a	DET
eurjchem-2064	195	33	wide	wide	ADJ
eurjchem-2064	195	34	range	range	NOUN
eurjchem-2064	195	35	of	of	ADP
eurjchem-2064	195	36	amines	amine	NOUN
eurjchem-2064	195	37	.	.	PUNCT
eurjchem-2064	196	1	upon	upon	SCONJ
eurjchem-2064	196	2	further	further	ADJ
eurjchem-2064	196	3	analysis	analysis	NOUN
eurjchem-2064	196	4	of	of	ADP
eurjchem-2064	196	5	the	the	DET
eurjchem-2064	196	6	results	result	NOUN
eurjchem-2064	196	7	,	,	PUNCT
eurjchem-2064	196	8	no	no	DET
eurjchem-2064	196	9	significant	significant	ADJ
eurjchem-2064	196	10	trend	trend	NOUN
eurjchem-2064	196	11	relating	relate	VERB
eurjchem-2064	196	12	substrate	substrate	NOUN
eurjchem-2064	196	13	and	and	CCONJ
eurjchem-2064	196	14	product	product	NOUN
eurjchem-2064	196	15	yield	yield	NOUN
eurjchem-2064	196	16	was	be	AUX
eurjchem-2064	196	17	noted	note	VERB
eurjchem-2064	196	18	,	,	PUNCT
eurjchem-2064	196	19	suggesting	suggest	VERB
eurjchem-2064	196	20	steric	steric	ADJ
eurjchem-2064	196	21	and	and	CCONJ
eurjchem-2064	196	22	electronic	electronic	ADJ
eurjchem-2064	196	23	effects	effect	NOUN
eurjchem-2064	196	24	were	be	AUX
eurjchem-2064	196	25	not	not	PART
eurjchem-2064	196	26	the	the	DET
eurjchem-2064	196	27	only	only	ADJ
eurjchem-2064	196	28	factors	factor	NOUN
eurjchem-2064	196	29	involved	involve	VERB
eurjchem-2064	196	30	.	.	PUNCT
eurjchem-2064	197	1	the	the	DET
eurjchem-2064	197	2	results	result	NOUN
eurjchem-2064	197	3	are	be	AUX
eurjchem-2064	197	4	,	,	PUNCT
eurjchem-2064	197	5	to	to	ADP
eurjchem-2064	197	6	some	some	DET
eurjchem-2064	197	7	extent	extent	NOUN
eurjchem-2064	197	8	,	,	PUNCT
eurjchem-2064	197	9	dependent	dependent	ADJ
eurjchem-2064	197	10	on	on	ADP
eurjchem-2064	197	11	differences	difference	NOUN
eurjchem-2064	197	12	in	in	ADP
eurjchem-2064	197	13	product	product	NOUN
eurjchem-2064	197	14	solubility	solubility	NOUN
eurjchem-2064	197	15	and	and	CCONJ
eurjchem-2064	197	16	methods	method	NOUN
eurjchem-2064	197	17	of	of	ADP
eurjchem-2064	197	18	isolation	isolation	NOUN
eurjchem-2064	197	19	/	/	SYM
eurjchem-2064	197	20	recrystallization	recrystallization	NOUN
eurjchem-2064	197	21	,	,	PUNCT
eurjchem-2064	197	22	which	which	PRON
eurjchem-2064	197	23	could	could	AUX
eurjchem-2064	197	24	explain	explain	VERB
eurjchem-2064	197	25	the	the	DET
eurjchem-2064	197	26	absence	absence	NOUN
eurjchem-2064	197	27	of	of	ADP
eurjchem-2064	197	28	any	any	DET
eurjchem-2064	197	29	trend	trend	NOUN
eurjchem-2064	197	30	.	.	PUNCT
eurjchem-2064	198	1	3.2	3.2	NUM
eurjchem-2064	198	2	.	.	PUNCT
eurjchem-2064	199	1	isolation	isolation	NOUN
eurjchem-2064	199	2	and	and	CCONJ
eurjchem-2064	199	3	recrystallization	recrystallization	NOUN
eurjchem-2064	199	4	methods	method	NOUN
eurjchem-2064	199	5	of	of	ADP
eurjchem-2064	199	6	isolation	isolation	NOUN
eurjchem-2064	199	7	varied	varied	ADJ
eurjchem-2064	199	8	depending	depend	VERB
eurjchem-2064	199	9	on	on	ADP
eurjchem-2064	199	10	the	the	DET
eurjchem-2064	199	11	starting	start	VERB
eurjchem-2064	199	12	materials	material	NOUN
eurjchem-2064	199	13	and	and	CCONJ
eurjchem-2064	199	14	conditions	condition	NOUN
eurjchem-2064	199	15	used	use	VERB
eurjchem-2064	199	16	.	.	PUNCT
eurjchem-2064	200	1	all	all	DET
eurjchem-2064	200	2	methods	method	NOUN
eurjchem-2064	200	3	described	describe	VERB
eurjchem-2064	200	4	herein	herein	NOUN
eurjchem-2064	200	5	were	be	AUX
eurjchem-2064	200	6	carried	carry	VERB
eurjchem-2064	200	7	out	out	ADP
eurjchem-2064	200	8	after	after	ADP
eurjchem-2064	200	9	acidification	acidification	NOUN
eurjchem-2064	200	10	of	of	ADP
eurjchem-2064	200	11	the	the	DET
eurjchem-2064	200	12	reaction	reaction	NOUN
eurjchem-2064	200	13	mixture	mixture	NOUN
eurjchem-2064	200	14	.	.	PUNCT
eurjchem-2064	201	1	primary	primary	ADJ
eurjchem-2064	201	2	amine	amine	ADJ
eurjchem-2064	201	3	derived	derive	VERB
eurjchem-2064	201	4	sulfonamides	sulfonamide	NOUN
eurjchem-2064	201	5	or	or	CCONJ
eurjchem-2064	201	6	sulfonamides	sulfonamide	NOUN
eurjchem-2064	201	7	synthesized	synthesize	VERB
eurjchem-2064	201	8	in	in	ADP
eurjchem-2064	201	9	the	the	DET
eurjchem-2064	201	10	presence	presence	NOUN
eurjchem-2064	201	11	of	of	ADP
eurjchem-2064	201	12	dichloromethane	dichloromethane	NOUN
eurjchem-2064	201	13	and	and	CCONJ
eurjchem-2064	201	14	pyridine	pyridine	ADJ
eurjchem-2064	201	15	underwent	underwent	NOUN
eurjchem-2064	201	16	extraction	extraction	NOUN
eurjchem-2064	201	17	with	with	ADP
eurjchem-2064	201	18	dichloromethane	dichloromethane	NOUN
eurjchem-2064	201	19	to	to	PART
eurjchem-2064	201	20	afford	afford	VERB
eurjchem-2064	201	21	the	the	DET
eurjchem-2064	201	22	crude	crude	ADJ
eurjchem-2064	201	23	product	product	NOUN
eurjchem-2064	201	24	.	.	PUNCT
eurjchem-2064	202	1	stenfors	stenfor	NOUN
eurjchem-2064	202	2	and	and	CCONJ
eurjchem-2064	202	3	ngassa	ngassa	NOUN
eurjchem-2064	202	4	/	/	SYM
eurjchem-2064	202	5	european	european	ADJ
eurjchem-2064	202	6	journal	journal	PROPN
eurjchem-2064	202	7	of	of	ADP
eurjchem-2064	202	8	chemistry	chemistry	NOUN
eurjchem-2064	202	9	12	12	NUM
eurjchem-2064	202	10	(	(	PUNCT
eurjchem-2064	202	11	2	2	NUM
eurjchem-2064	202	12	)	)	PUNCT
eurjchem-2064	202	13	(	(	PUNCT
eurjchem-2064	202	14	2021	2021	NUM
eurjchem-2064	202	15	)	)	PUNCT
eurjchem-2064	202	16	109	109	NUM
eurjchem-2064	202	17	-	-	SYM
eurjchem-2064	202	18	116	116	NUM
eurjchem-2064	202	19	113	113	NUM
eurjchem-2064	202	20	2021	2021	NUM
eurjchem-2064	202	21	–	–	PUNCT
eurjchem-2064	202	22	european	european	ADJ
eurjchem-2064	202	23	journal	journal	NOUN
eurjchem-2064	202	24	of	of	ADP
eurjchem-2064	202	25	chemistry	chemistry	NOUN
eurjchem-2064	202	26	–	–	PUNCT
eurjchem-2064	202	27	cc	cc	NOUN
eurjchem-2064	202	28	by	by	ADP
eurjchem-2064	202	29	nc	nc	PROPN
eurjchem-2064	202	30	–	–	PUNCT
eurjchem-2064	202	31	doi	doi	NOUN
eurjchem-2064	202	32	:	:	PUNCT
eurjchem-2064	202	33	10.5155	10.5155	NUM
eurjchem-2064	202	34	/	/	SYM
eurjchem-2064	202	35	eurjchem.12.2.109	eurjchem.12.2.109	NUM
eurjchem-2064	202	36	-	-	PUNCT
eurjchem-2064	202	37	116.2064	116.2064	NUM
eurjchem-2064	202	38	table	table	NOUN
eurjchem-2064	202	39	2	2	NUM
eurjchem-2064	202	40	.	.	PUNCT
eurjchem-2064	202	41	base	base	NOUN
eurjchem-2064	202	42	and	and	CCONJ
eurjchem-2064	202	43	solvent	solvent	ADJ
eurjchem-2064	202	44	effects	effect	NOUN
eurjchem-2064	202	45	in	in	ADP
eurjchem-2064	202	46	the	the	DET
eurjchem-2064	202	47	synthesis	synthesis	NOUN
eurjchem-2064	202	48	of	of	ADP
eurjchem-2064	202	49	n	n	X
eurjchem-2064	202	50	-	-	PUNCT
eurjchem-2064	202	51	butyl-4	butyl-4	NOUN
eurjchem-2064	202	52	-	-	PUNCT
eurjchem-2064	202	53	methylbenzenesulfonamide	methylbenzenesulfonamide	NOUN
eurjchem-2064	202	54	a	a	DET
eurjchem-2064	202	55	(	(	PUNCT
eurjchem-2064	202	56	4	4	NUM
eurjchem-2064	202	57	)	)	PUNCT
eurjchem-2064	202	58	.	.	PUNCT
eurjchem-2064	203	1	entries	entry	NOUN
eurjchem-2064	203	2	are	be	AUX
eurjchem-2064	203	3	presented	present	VERB
eurjchem-2064	203	4	in	in	ADP
eurjchem-2064	203	5	order	order	NOUN
eurjchem-2064	203	6	of	of	ADP
eurjchem-2064	203	7	decreasing	decrease	VERB
eurjchem-2064	203	8	yield	yield	NOUN
eurjchem-2064	203	9	.	.	PUNCT
eurjchem-2064	204	1	s	s	PART
eurjchem-2064	204	2	o	o	X
eurjchem-2064	204	3	o	o	X
eurjchem-2064	204	4	cl	cl	NOUN
eurjchem-2064	205	1	+	+	CCONJ
eurjchem-2064	205	2	s	s	X
eurjchem-2064	205	3	o	o	NOUN
eurjchem-2064	205	4	o	o	NOUN
eurjchem-2064	205	5	n	n	CCONJ
eurjchem-2064	205	6	base	base	NOUN
eurjchem-2064	205	7	solvent	solvent	ADJ
eurjchem-2064	205	8	h	h	NOUN
eurjchem-2064	205	9	h2n	h2n	PROPN
eurjchem-2064	205	10	entry	entry	NOUN
eurjchem-2064	205	11	base	base	NOUN
eurjchem-2064	205	12	solvent	solvent	NOUN
eurjchem-2064	205	13	yield	yield	NOUN
eurjchem-2064	205	14	(	(	PUNCT
eurjchem-2064	205	15	%	%	NOUN
eurjchem-2064	205	16	)	)	PUNCT
eurjchem-2064	205	17	1	1	NUM
eurjchem-2064	205	18	c	c	NOUN
eurjchem-2064	205	19	0.59	0.59	NUM
eurjchem-2064	205	20	m	m	NOUN
eurjchem-2064	205	21	aq	aq	NOUN
eurjchem-2064	205	22	.	.	PUNCT
eurjchem-2064	205	23	k2co3	k2co3	ADJ
eurjchem-2064	205	24	thf	thf	NOUN
eurjchem-2064	205	25	90	90	NUM
eurjchem-2064	205	26	2	2	NUM
eurjchem-2064	205	27	c	c	NOUN
eurjchem-2064	205	28	0.59	0.59	NUM
eurjchem-2064	205	29	m	m	NOUN
eurjchem-2064	205	30	aq	aq	NOUN
eurjchem-2064	205	31	.	.	PUNCT
eurjchem-2064	205	32	k2co3	k2co3	ADJ
eurjchem-2064	205	33	acetone	acetone	NOUN
eurjchem-2064	205	34	82	82	NUM
eurjchem-2064	205	35	3	3	NUM
eurjchem-2064	205	36	c	c	NOUN
eurjchem-2064	205	37	0.59	0.59	NUM
eurjchem-2064	205	38	m	m	NOUN
eurjchem-2064	205	39	aq	aq	NOUN
eurjchem-2064	205	40	.	.	PUNCT
eurjchem-2064	205	41	k2co3	k2co3	ADJ
eurjchem-2064	205	42	ethanol	ethanol	NOUN
eurjchem-2064	205	43	80	80	NUM
eurjchem-2064	205	44	4	4	NUM
eurjchem-2064	205	45	d	d	SYM
eurjchem-2064	205	46	1.2	1.2	NUM
eurjchem-2064	205	47	m	m	NOUN
eurjchem-2064	205	48	aq	aq	NOUN
eurjchem-2064	205	49	.	.	PUNCT
eurjchem-2064	205	50	k2co3	k2co3	ADJ
eurjchem-2064	205	51	thf	thf	NOUN
eurjchem-2064	205	52	77	77	NUM
eurjchem-2064	205	53	5	5	NUM
eurjchem-2064	205	54	c	c	NOUN
eurjchem-2064	205	55	0.59	0.59	NUM
eurjchem-2064	205	56	m	m	NOUN
eurjchem-2064	205	57	aq	aq	NOUN
eurjchem-2064	205	58	.	.	PUNCT
eurjchem-2064	206	1	naoh	naoh	NOUN
eurjchem-2064	206	2	thf	thf	NOUN
eurjchem-2064	206	3	69	69	NUM
eurjchem-2064	206	4	6	6	NUM
eurjchem-2064	206	5	b	b	PROPN
eurjchem-2064	206	6	pyridine	pyridine	ADJ
eurjchem-2064	206	7	dcm	dcm	NOUN
eurjchem-2064	206	8	54	54	NUM
eurjchem-2064	206	9	a	a	DET
eurjchem-2064	206	10	reaction	reaction	NOUN
eurjchem-2064	206	11	conditions	condition	NOUN
eurjchem-2064	206	12	:	:	PUNCT
eurjchem-2064	206	13	reaction	reaction	NOUN
eurjchem-2064	206	14	conditions	condition	NOUN
eurjchem-2064	206	15	:	:	PUNCT
eurjchem-2064	206	16	4	4	NUM
eurjchem-2064	206	17	-	-	PUNCT
eurjchem-2064	206	18	methylbenzenesulfonyl	methylbenzenesulfonyl	NOUN
eurjchem-2064	206	19	chloride	chloride	NOUN
eurjchem-2064	206	20	(	(	PUNCT
eurjchem-2064	206	21	5.25	5.25	NUM
eurjchem-2064	206	22	mmol	mmol	NOUN
eurjchem-2064	206	23	,	,	PUNCT
eurjchem-2064	206	24	1.0	1.0	NUM
eurjchem-2064	206	25	eq	eq	NOUN
eurjchem-2064	206	26	)	)	PUNCT
eurjchem-2064	206	27	was	be	AUX
eurjchem-2064	206	28	dissolved	dissolve	VERB
eurjchem-2064	206	29	in	in	ADP
eurjchem-2064	206	30	solvent	solvent	NOUN
eurjchem-2064	206	31	,	,	PUNCT
eurjchem-2064	206	32	followed	follow	VERB
eurjchem-2064	206	33	by	by	ADP
eurjchem-2064	206	34	the	the	DET
eurjchem-2064	206	35	dropwise	dropwise	NOUN
eurjchem-2064	206	36	addition	addition	NOUN
eurjchem-2064	206	37	of	of	ADP
eurjchem-2064	206	38	butylamine	butylamine	NOUN
eurjchem-2064	206	39	(	(	PUNCT
eurjchem-2064	206	40	5.90	5.90	NUM
eurjchem-2064	206	41	mmol	mmol	NOUN
eurjchem-2064	206	42	,	,	PUNCT
eurjchem-2064	206	43	1.125	1.125	NUM
eurjchem-2064	206	44	eq	eq	NOUN
eurjchem-2064	206	45	)	)	PUNCT
eurjchem-2064	206	46	and	and	CCONJ
eurjchem-2064	206	47	base	base	NOUN
eurjchem-2064	206	48	(	(	PUNCT
eurjchem-2064	206	49	5.90	5.90	NUM
eurjchem-2064	206	50	mmol	mmol	NOUN
eurjchem-2064	206	51	,	,	PUNCT
eurjchem-2064	206	52	1.125	1.125	NUM
eurjchem-2064	206	53	eq	eq	NOUN
eurjchem-2064	206	54	)	)	PUNCT
eurjchem-2064	206	55	.	.	PUNCT
eurjchem-2064	207	1	reactions	reaction	NOUN
eurjchem-2064	207	2	were	be	AUX
eurjchem-2064	207	3	run	run	VERB
eurjchem-2064	207	4	at	at	ADP
eurjchem-2064	207	5	room	room	NOUN
eurjchem-2064	207	6	temperature	temperature	NOUN
eurjchem-2064	207	7	for	for	ADP
eurjchem-2064	207	8	24	24	NUM
eurjchem-2064	207	9	hours	hour	NOUN
eurjchem-2064	207	10	.	.	PUNCT
eurjchem-2064	208	1	b	b	X
eurjchem-2064	208	2	reaction	reaction	NOUN
eurjchem-2064	208	3	run	run	VERB
eurjchem-2064	208	4	under	under	ADP
eurjchem-2064	208	5	nitrogen	nitrogen	NOUN
eurjchem-2064	208	6	atmosphere	atmosphere	NOUN
eurjchem-2064	208	7	;	;	PUNCT
eurjchem-2064	208	8	10	10	NUM
eurjchem-2064	208	9	ml	ml	NOUN
eurjchem-2064	208	10	of	of	ADP
eurjchem-2064	208	11	solvent	solvent	NOUN
eurjchem-2064	208	12	.	.	PUNCT
eurjchem-2064	209	1	c	c	NOUN
eurjchem-2064	209	2	10	10	NUM
eurjchem-2064	209	3	ml	ml	NOUN
eurjchem-2064	209	4	of	of	ADP
eurjchem-2064	209	5	aqueous	aqueous	ADJ
eurjchem-2064	209	6	base	base	NOUN
eurjchem-2064	209	7	;	;	PUNCT
eurjchem-2064	209	8	10	10	NUM
eurjchem-2064	209	9	ml	ml	NOUN
eurjchem-2064	209	10	of	of	ADP
eurjchem-2064	209	11	solvent	solvent	NOUN
eurjchem-2064	209	12	.	.	PUNCT
eurjchem-2064	210	1	d	d	ADP
eurjchem-2064	210	2	5	5	NUM
eurjchem-2064	210	3	ml	ml	NOUN
eurjchem-2064	210	4	of	of	ADP
eurjchem-2064	210	5	aqueous	aqueous	ADJ
eurjchem-2064	210	6	base	base	NOUN
eurjchem-2064	210	7	;	;	PUNCT
eurjchem-2064	210	8	5	5	NUM
eurjchem-2064	210	9	ml	ml	NOUN
eurjchem-2064	210	10	of	of	ADP
eurjchem-2064	210	11	solvent	solvent	NOUN
eurjchem-2064	210	12	.	.	PUNCT
eurjchem-2064	211	1	(	(	PUNCT
eurjchem-2064	211	2	1	1	X
eurjchem-2064	211	3	)	)	PUNCT
eurjchem-2064	211	4	(	(	PUNCT
eurjchem-2064	211	5	2	2	NUM
eurjchem-2064	211	6	)	)	PUNCT
eurjchem-2064	211	7	(	(	PUNCT
eurjchem-2064	211	8	5	5	NUM
eurjchem-2064	211	9	)	)	PUNCT
eurjchem-2064	211	10	(	(	PUNCT
eurjchem-2064	211	11	4	4	NUM
eurjchem-2064	211	12	)	)	PUNCT
eurjchem-2064	211	13	(	(	PUNCT
eurjchem-2064	211	14	9	9	NUM
eurjchem-2064	211	15	)	)	PUNCT
eurjchem-2064	211	16	(	(	PUNCT
eurjchem-2064	211	17	11	11	NUM
eurjchem-2064	211	18	)	)	PUNCT
eurjchem-2064	211	19	(	(	PUNCT
eurjchem-2064	211	20	12	12	NUM
eurjchem-2064	211	21	)	)	PUNCT
eurjchem-2064	211	22	figure	figure	NOUN
eurjchem-2064	211	23	4	4	NUM
eurjchem-2064	211	24	.	.	PUNCT
eurjchem-2064	212	1	the	the	DET
eurjchem-2064	212	2	structure	structure	NOUN
eurjchem-2064	212	3	of	of	ADP
eurjchem-2064	212	4	n	n	CCONJ
eurjchem-2064	212	5	-	-	PUNCT
eurjchem-2064	212	6	benzyl	benzyl	NOUN
eurjchem-2064	212	7	-	-	PUNCT
eurjchem-2064	212	8	n,4	n,4	DET
eurjchem-2064	212	9	-	-	PUNCT
eurjchem-2064	212	10	dimethylbenzenesulfonamide	dimethylbenzenesulfonamide	NOUN
eurjchem-2064	212	11	(	(	PUNCT
eurjchem-2064	212	12	1	1	NUM
eurjchem-2064	212	13	)	)	PUNCT
eurjchem-2064	212	14	,	,	PUNCT
eurjchem-2064	212	15	4-[(4	4-[(4	NOUN
eurjchem-2064	212	16	-	-	PUNCT
eurjchem-2064	212	17	methylbenzene)sulfonyl]morpholine	methylbenzene)sulfonyl]morpholine	X
eurjchem-2064	212	18	(	(	PUNCT
eurjchem-2064	212	19	2	2	NUM
eurjchem-2064	212	20	)	)	PUNCT
eurjchem-2064	212	21	,	,	PUNCT
eurjchem-2064	212	22	n	n	CCONJ
eurjchem-2064	212	23	-	-	PUNCT
eurjchem-2064	212	24	butyl-4	butyl-4	NOUN
eurjchem-2064	212	25	-	-	PUNCT
eurjchem-2064	212	26	methylbenzenesulfonamide	methylbenzenesulfonamide	NOUN
eurjchem-2064	212	27	(	(	PUNCT
eurjchem-2064	212	28	4	4	NUM
eurjchem-2064	212	29	)	)	PUNCT
eurjchem-2064	212	30	,	,	PUNCT
eurjchem-2064	212	31	1-[(4	1-[(4	NOUN
eurjchem-2064	212	32	-	-	PUNCT
eurjchem-2064	212	33	methylbenzene)sulfonyl]piperidine	methylbenzene)sulfonyl]piperidine	NOUN
eurjchem-2064	212	34	(	(	PUNCT
eurjchem-2064	212	35	5	5	NUM
eurjchem-2064	212	36	)	)	PUNCT
eurjchem-2064	212	37	,	,	PUNCT
eurjchem-2064	212	38	4	4	NUM
eurjchem-2064	212	39	-	-	PUNCT
eurjchem-2064	212	40	methyl	methyl	NOUN
eurjchem-2064	212	41	-	-	PUNCT
eurjchem-2064	212	42	n	n	CCONJ
eurjchem-2064	212	43	-	-	PUNCT
eurjchem-2064	212	44	phenylbenzenesulfonamide	phenylbenzenesulfonamide	NOUN
eurjchem-2064	212	45	(	(	PUNCT
eurjchem-2064	212	46	9	9	NUM
eurjchem-2064	212	47	)	)	PUNCT
eurjchem-2064	212	48	,	,	PUNCT
eurjchem-2064	212	49	n	n	CCONJ
eurjchem-2064	212	50	,	,	PUNCT
eurjchem-2064	212	51	n	n	CCONJ
eurjchem-2064	212	52	-	-	PUNCT
eurjchem-2064	212	53	bis(2	bis(2	NOUN
eurjchem-2064	212	54	-	-	PUNCT
eurjchem-2064	212	55	hydroxyethyl)-4	hydroxyethyl)-4	NOUN
eurjchem-2064	212	56	-	-	PUNCT
eurjchem-2064	212	57	methylbenzenesulfonamide	methylbenzenesulfonamide	NOUN
eurjchem-2064	212	58	(	(	PUNCT
eurjchem-2064	212	59	11	11	NUM
eurjchem-2064	212	60	)	)	PUNCT
eurjchem-2064	212	61	and	and	CCONJ
eurjchem-2064	212	62	4	4	NUM
eurjchem-2064	212	63	-	-	PUNCT
eurjchem-2064	212	64	methyl	methyl	NOUN
eurjchem-2064	212	65	-	-	PUNCT
eurjchem-2064	212	66	n-(2,4,4	n-(2,4,4	VERB
eurjchem-2064	212	67	-	-	PUNCT
eurjchem-2064	212	68	trimethylpentan-2	trimethylpentan-2	NOUN
eurjchem-2064	212	69	-	-	PUNCT
eurjchem-2064	212	70	yl)benzenesulfonamide	yl)benzenesulfonamide	NOUN
eurjchem-2064	212	71	(	(	PUNCT
eurjchem-2064	212	72	12	12	NUM
eurjchem-2064	212	73	)	)	PUNCT
eurjchem-2064	212	74	elucidated	elucidate	VERB
eurjchem-2064	212	75	by	by	ADP
eurjchem-2064	212	76	x	x	ADJ
eurjchem-2064	212	77	-	-	NOUN
eurjchem-2064	212	78	ray	ray	NOUN
eurjchem-2064	212	79	diffraction	diffraction	NOUN
eurjchem-2064	212	80	at	at	ADP
eurjchem-2064	212	81	173	173	NUM
eurjchem-2064	212	82	k	k	NOUN
eurjchem-2064	212	83	with	with	ADP
eurjchem-2064	212	84	atom	atom	NOUN
eurjchem-2064	212	85	labeling	labeling	NOUN
eurjchem-2064	212	86	schemes	scheme	NOUN
eurjchem-2064	212	87	.	.	PUNCT
eurjchem-2064	213	1	displacement	displacement	NOUN
eurjchem-2064	213	2	of	of	ADP
eurjchem-2064	213	3	ellipsoids	ellipsoid	NOUN
eurjchem-2064	213	4	is	be	AUX
eurjchem-2064	213	5	shown	show	VERB
eurjchem-2064	213	6	at	at	ADP
eurjchem-2064	213	7	the	the	DET
eurjchem-2064	213	8	50	50	NUM
eurjchem-2064	213	9	%	%	NOUN
eurjchem-2064	213	10	probability	probability	NOUN
eurjchem-2064	213	11	level	level	NOUN
eurjchem-2064	213	12	.	.	PUNCT
eurjchem-2064	214	1	hydrogen	hydrogen	NOUN
eurjchem-2064	214	2	atoms	atom	NOUN
eurjchem-2064	214	3	have	have	AUX
eurjchem-2064	214	4	been	be	AUX
eurjchem-2064	214	5	omitted	omit	VERB
eurjchem-2064	214	6	for	for	ADP
eurjchem-2064	214	7	clarity	clarity	NOUN
eurjchem-2064	214	8	.	.	PUNCT
eurjchem-2064	215	1	secondary	secondary	ADJ
eurjchem-2064	215	2	or	or	CCONJ
eurjchem-2064	215	3	heterocyclic	heterocyclic	ADJ
eurjchem-2064	215	4	amine	amine	ADJ
eurjchem-2064	215	5	derived	derive	VERB
eurjchem-2064	215	6	sulfonamides	sulfonamide	NOUN
eurjchem-2064	215	7	synthesized	synthesize	VERB
eurjchem-2064	215	8	in	in	ADP
eurjchem-2064	215	9	a	a	DET
eurjchem-2064	215	10	biphasic	biphasic	ADJ
eurjchem-2064	215	11	system	system	NOUN
eurjchem-2064	215	12	were	be	AUX
eurjchem-2064	215	13	isolated	isolate	VERB
eurjchem-2064	215	14	directly	directly	ADV
eurjchem-2064	215	15	from	from	ADP
eurjchem-2064	215	16	the	the	DET
eurjchem-2064	215	17	reaction	reaction	NOUN
eurjchem-2064	215	18	mixture	mixture	NOUN
eurjchem-2064	215	19	.	.	PUNCT
eurjchem-2064	216	1	primary	primary	ADJ
eurjchem-2064	216	2	amine	amine	ADJ
eurjchem-2064	216	3	derived	derive	VERB
eurjchem-2064	216	4	sulfonamides	sulfonamide	NOUN
eurjchem-2064	216	5	gave	give	VERB
eurjchem-2064	216	6	crude	crude	ADJ
eurjchem-2064	216	7	products	product	NOUN
eurjchem-2064	216	8	as	as	ADP
eurjchem-2064	216	9	liquids	liquid	NOUN
eurjchem-2064	216	10	or	or	CCONJ
eurjchem-2064	216	11	amorphous	amorphous	ADJ
eurjchem-2064	216	12	solids	solid	NOUN
eurjchem-2064	216	13	.	.	PUNCT
eurjchem-2064	217	1	solid	solid	ADJ
eurjchem-2064	217	2	crude	crude	ADJ
eurjchem-2064	217	3	products	product	NOUN
eurjchem-2064	217	4	were	be	AUX
eurjchem-2064	217	5	regularly	regularly	ADV
eurjchem-2064	217	6	obtained	obtain	VERB
eurjchem-2064	217	7	with	with	ADP
eurjchem-2064	217	8	the	the	DET
eurjchem-2064	217	9	use	use	NOUN
eurjchem-2064	217	10	of	of	ADP
eurjchem-2064	217	11	secondary	secondary	ADJ
eurjchem-2064	217	12	or	or	CCONJ
eurjchem-2064	217	13	heterocyclic	heterocyclic	ADJ
eurjchem-2064	217	14	amines	amine	NOUN
eurjchem-2064	217	15	.	.	PUNCT
eurjchem-2064	218	1	the	the	DET
eurjchem-2064	218	2	crude	crude	ADJ
eurjchem-2064	218	3	products	product	NOUN
eurjchem-2064	218	4	underwent	undergo	VERB
eurjchem-2064	218	5	different	different	ADJ
eurjchem-2064	218	6	methods	method	NOUN
eurjchem-2064	218	7	of	of	ADP
eurjchem-2064	218	8	recrystallization	recrystallization	NOUN
eurjchem-2064	218	9	depending	depend	VERB
eurjchem-2064	218	10	on	on	ADP
eurjchem-2064	218	11	their	their	PRON
eurjchem-2064	218	12	state	state	NOUN
eurjchem-2064	218	13	.	.	PUNCT
eurjchem-2064	219	1	liquid	liquid	ADJ
eurjchem-2064	219	2	and	and	CCONJ
eurjchem-2064	219	3	amorphous	amorphous	ADJ
eurjchem-2064	219	4	solid	solid	ADJ
eurjchem-2064	219	5	products	product	NOUN
eurjchem-2064	219	6	were	be	AUX
eurjchem-2064	219	7	dried	dry	VERB
eurjchem-2064	219	8	under	under	ADP
eurjchem-2064	219	9	vacuum	vacuum	NOUN
eurjchem-2064	219	10	and	and	CCONJ
eurjchem-2064	219	11	triturated	triturate	VERB
eurjchem-2064	219	12	with	with	ADP
eurjchem-2064	219	13	either	either	CCONJ
eurjchem-2064	219	14	chilled	chilled	ADJ
eurjchem-2064	219	15	diethyl	diethyl	NOUN
eurjchem-2064	219	16	ether	ether	NOUN
eurjchem-2064	219	17	,	,	PUNCT
eurjchem-2064	219	18	hexanes	hexane	NOUN
eurjchem-2064	219	19	,	,	PUNCT
eurjchem-2064	219	20	or	or	CCONJ
eurjchem-2064	219	21	petroleum	petroleum	NOUN
eurjchem-2064	219	22	ether	ether	NOUN
eurjchem-2064	219	23	to	to	PART
eurjchem-2064	219	24	give	give	VERB
eurjchem-2064	219	25	a	a	DET
eurjchem-2064	219	26	solid	solid	NOUN
eurjchem-2064	219	27	.	.	PUNCT
eurjchem-2064	220	1	the	the	DET
eurjchem-2064	220	2	solid	solid	ADJ
eurjchem-2064	220	3	products	product	NOUN
eurjchem-2064	220	4	were	be	AUX
eurjchem-2064	220	5	then	then	ADV
eurjchem-2064	220	6	recrystallized	recrystallize	VERB
eurjchem-2064	220	7	in	in	ADP
eurjchem-2064	220	8	ethanol	ethanol	NOUN
eurjchem-2064	220	9	and	and	CCONJ
eurjchem-2064	220	10	chilled	chill	VERB
eurjchem-2064	220	11	at	at	ADP
eurjchem-2064	220	12	0	0	NUM
eurjchem-2064	220	13	°	°	ADP
eurjchem-2064	220	14	c	c	NOUN
eurjchem-2064	220	15	to	to	PART
eurjchem-2064	220	16	afford	afford	VERB
eurjchem-2064	220	17	highly	highly	ADV
eurjchem-2064	220	18	pure	pure	ADJ
eurjchem-2064	220	19	products	product	NOUN
eurjchem-2064	220	20	.	.	PUNCT
eurjchem-2064	221	1	the	the	DET
eurjchem-2064	221	2	dropwise	dropwise	NOUN
eurjchem-2064	221	3	addition	addition	NOUN
eurjchem-2064	221	4	of	of	ADP
eurjchem-2064	221	5	chilled	chill	VERB
eurjchem-2064	221	6	petroleum	petroleum	NOUN
eurjchem-2064	221	7	ether	ether	NOUN
eurjchem-2064	221	8	or	or	CCONJ
eurjchem-2064	221	9	hexane	hexane	NOUN
eurjchem-2064	221	10	was	be	AUX
eurjchem-2064	221	11	occasionally	occasionally	ADV
eurjchem-2064	221	12	employed	employ	VERB
eurjchem-2064	221	13	to	to	PART
eurjchem-2064	221	14	speed	speed	VERB
eurjchem-2064	221	15	up	up	ADP
eurjchem-2064	221	16	recrystallization	recrystallization	NOUN
eurjchem-2064	221	17	.	.	PUNCT
eurjchem-2064	222	1	3.3	3.3	NUM
eurjchem-2064	222	2	.	.	PUNCT
eurjchem-2064	222	3	crystallographic	crystallographic	ADJ
eurjchem-2064	222	4	characterization	characterization	NOUN
eurjchem-2064	222	5	the	the	DET
eurjchem-2064	222	6	crystal	crystal	NOUN
eurjchem-2064	222	7	structures	structure	NOUN
eurjchem-2064	222	8	of	of	ADP
eurjchem-2064	222	9	five	five	NUM
eurjchem-2064	222	10	novel	novel	ADJ
eurjchem-2064	222	11	compounds	compound	NOUN
eurjchem-2064	222	12	,	,	PUNCT
eurjchem-2064	222	13	and	and	CCONJ
eurjchem-2064	222	14	two	two	NUM
eurjchem-2064	222	15	packing	packing	NOUN
eurjchem-2064	222	16	polymorphs	polymorph	NOUN
eurjchem-2064	222	17	of	of	ADP
eurjchem-2064	222	18	existing	exist	VERB
eurjchem-2064	222	19	structures	structure	NOUN
eurjchem-2064	222	20	were	be	AUX
eurjchem-2064	222	21	obtained	obtain	VERB
eurjchem-2064	222	22	through	through	ADP
eurjchem-2064	222	23	single	single	ADJ
eurjchem-2064	222	24	-	-	PUNCT
eurjchem-2064	222	25	crystal	crystal	NOUN
eurjchem-2064	222	26	x	x	ADJ
eurjchem-2064	222	27	-	-	NOUN
eurjchem-2064	222	28	ray	ray	NOUN
eurjchem-2064	222	29	diffraction	diffraction	NOUN
eurjchem-2064	222	30	experiments	experiment	NOUN
eurjchem-2064	222	31	(	(	PUNCT
eurjchem-2064	222	32	figure	figure	NOUN
eurjchem-2064	222	33	4	4	NUM
eurjchem-2064	222	34	)	)	PUNCT
eurjchem-2064	222	35	.	.	PUNCT
eurjchem-2064	223	1	114	114	NUM
eurjchem-2064	223	2	stenfors	stenfor	NOUN
eurjchem-2064	223	3	and	and	CCONJ
eurjchem-2064	223	4	ngassa	ngassa	NOUN
eurjchem-2064	223	5	/	/	SYM
eurjchem-2064	223	6	european	european	ADJ
eurjchem-2064	223	7	journal	journal	PROPN
eurjchem-2064	223	8	of	of	ADP
eurjchem-2064	223	9	chemistry	chemistry	NOUN
eurjchem-2064	223	10	12	12	NUM
eurjchem-2064	223	11	(	(	PUNCT
eurjchem-2064	223	12	2	2	NUM
eurjchem-2064	223	13	)	)	PUNCT
eurjchem-2064	223	14	(	(	PUNCT
eurjchem-2064	223	15	2021	2021	NUM
eurjchem-2064	223	16	)	)	PUNCT
eurjchem-2064	223	17	109	109	NUM
eurjchem-2064	223	18	-	-	SYM
eurjchem-2064	223	19	116	116	NUM
eurjchem-2064	223	20	2021	2021	NUM
eurjchem-2064	223	21	–	–	PUNCT
eurjchem-2064	223	22	european	european	ADJ
eurjchem-2064	223	23	journal	journal	NOUN
eurjchem-2064	223	24	of	of	ADP
eurjchem-2064	223	25	chemistry	chemistry	NOUN
eurjchem-2064	223	26	–	–	PUNCT
eurjchem-2064	223	27	cc	cc	NOUN
eurjchem-2064	223	28	by	by	ADP
eurjchem-2064	223	29	nc	nc	PROPN
eurjchem-2064	223	30	–	–	PUNCT
eurjchem-2064	223	31	doi	doi	NOUN
eurjchem-2064	223	32	:	:	PUNCT
eurjchem-2064	223	33	10.5155	10.5155	NUM
eurjchem-2064	223	34	/	/	SYM
eurjchem-2064	223	35	eurjchem.12.2.109	eurjchem.12.2.109	NUM
eurjchem-2064	223	36	-	-	PUNCT
eurjchem-2064	223	37	116.2064	116.2064	NUM
eurjchem-2064	223	38	table	table	NOUN
eurjchem-2064	223	39	3	3	NUM
eurjchem-2064	223	40	.	.	PUNCT
eurjchem-2064	223	41	data	datum	NOUN
eurjchem-2064	223	42	parameters	parameter	NOUN
eurjchem-2064	223	43	for	for	ADP
eurjchem-2064	223	44	the	the	DET
eurjchem-2064	223	45	crystal	crystal	NOUN
eurjchem-2064	223	46	lattices	lattice	NOUN
eurjchem-2064	223	47	of	of	ADP
eurjchem-2064	223	48	the	the	DET
eurjchem-2064	223	49	investigated	investigate	VERB
eurjchem-2064	223	50	sulfonamide	sulfonamide	NOUN
eurjchem-2064	223	51	derivatives	derivative	NOUN
eurjchem-2064	223	52	.	.	PUNCT
eurjchem-2064	224	1	compound	compound	NOUN
eurjchem-2064	224	2	1	1	NUM
eurjchem-2064	224	3	2	2	NUM
eurjchem-2064	224	4	4	4	NUM
eurjchem-2064	224	5	9	9	NUM
eurjchem-2064	224	6	molecular	molecular	ADJ
eurjchem-2064	224	7	formula	formula	NOUN
eurjchem-2064	224	8	c15h17no2s	c15h17no2s	PROPN
eurjchem-2064	224	9	c11h15no3s	c11h15no3s	PROPN
eurjchem-2064	224	10	c11h17no2s	c11h17no2s	PROPN
eurjchem-2064	224	11	c13h13no2s	c13h13no2s	PROPN
eurjchem-2064	224	12	crystal	crystal	NOUN
eurjchem-2064	224	13	system	system	NOUN
eurjchem-2064	224	14	monoclinic	monoclinic	ADJ
eurjchem-2064	224	15	monoclinic	monoclinic	ADJ
eurjchem-2064	224	16	monoclinic	monoclinic	ADJ
eurjchem-2064	224	17	monoclinic	monoclinic	ADJ
eurjchem-2064	224	18	space	space	NOUN
eurjchem-2064	224	19	group	group	NOUN
eurjchem-2064	224	20	p21	p21	PROPN
eurjchem-2064	224	21	/	/	SYM
eurjchem-2064	224	22	c	c	PROPN
eurjchem-2064	224	23	p21	p21	PROPN
eurjchem-2064	224	24	/	/	SYM
eurjchem-2064	224	25	c	c	PROPN
eurjchem-2064	224	26	p21	p21	PROPN
eurjchem-2064	224	27	/	/	SYM
eurjchem-2064	224	28	c	c	PROPN
eurjchem-2064	224	29	p21	p21	PROPN
eurjchem-2064	224	30	/	/	SYM
eurjchem-2064	224	31	c	c	PROPN
eurjchem-2064	225	1	mr	mr	PROPN
eurjchem-2064	225	2	275.37	275.37	NUM
eurjchem-2064	225	3	241.31	241.31	NUM
eurjchem-2064	225	4	227.31	227.31	NUM
eurjchem-2064	225	5	247.32	247.32	NUM
eurjchem-2064	225	6	a	a	DET
eurjchem-2064	225	7	(	(	PUNCT
eurjchem-2064	225	8	å	å	NOUN
eurjchem-2064	225	9	)	)	PUNCT
eurjchem-2064	225	10	15.0517(2	15.0517(2	NUM
eurjchem-2064	225	11	)	)	PUNCT
eurjchem-2064	225	12	8.0852(10	8.0852(10	NUM
eurjchem-2064	225	13	)	)	PUNCT
eurjchem-2064	225	14	7.85980(10	7.85980(10	NUM
eurjchem-2064	225	15	)	)	PUNCT
eurjchem-2064	225	16	8.6674(1	8.6674(1	NUM
eurjchem-2064	225	17	)	)	PUNCT
eurjchem-2064	225	18	b	b	X
eurjchem-2064	225	19	(	(	PUNCT
eurjchem-2064	225	20	å	å	NOUN
eurjchem-2064	225	21	)	)	PUNCT
eurjchem-2064	225	22	8.2817(1	8.2817(1	NUM
eurjchem-2064	225	23	)	)	PUNCT
eurjchem-2064	225	24	17.913(2	17.913(2	NUM
eurjchem-2064	225	25	)	)	PUNCT
eurjchem-2064	225	26	15.3377(2	15.3377(2	NUM
eurjchem-2064	225	27	)	)	PUNCT
eurjchem-2064	225	28	9.6925(1	9.6925(1	NUM
eurjchem-2064	225	29	)	)	PUNCT
eurjchem-2064	225	30	c	c	NOUN
eurjchem-2064	225	31	(	(	PUNCT
eurjchem-2064	225	32	å	å	NOUN
eurjchem-2064	225	33	)	)	PUNCT
eurjchem-2064	225	34	11.8484(2	11.8484(2	NUM
eurjchem-2064	225	35	)	)	PUNCT
eurjchem-2064	225	36	8.7501(11	8.7501(11	NUM
eurjchem-2064	225	37	)	)	PUNCT
eurjchem-2064	225	38	10.23190(10	10.23190(10	NUM
eurjchem-2064	225	39	)	)	PUNCT
eurjchem-2064	225	40	15.1001(2	15.1001(2	NUM
eurjchem-2064	225	41	)	)	PUNCT
eurjchem-2064	225	42	β	β	X
eurjchem-2064	225	43	(	(	PUNCT
eurjchem-2064	225	44	°	°	PROPN
eurjchem-2064	225	45	)	)	PUNCT
eurjchem-2064	225	46	107.1101(9	107.1101(9	NUM
eurjchem-2064	225	47	)	)	PUNCT
eurjchem-2064	225	48	111.2125(14	111.2125(14	NUM
eurjchem-2064	225	49	)	)	PUNCT
eurjchem-2064	225	50	106.5662(8	106.5662(8	NUM
eurjchem-2064	225	51	)	)	PUNCT
eurjchem-2064	225	52	98.8679(7	98.8679(7	NUM
eurjchem-2064	225	53	)	)	PUNCT
eurjchem-2064	225	54	volume	volume	NOUN
eurjchem-2064	225	55	(	(	PUNCT
eurjchem-2064	225	56	å3	å3	PROPN
eurjchem-2064	225	57	)	)	PUNCT
eurjchem-2064	225	58	1411.58(4	1411.58(4	NUM
eurjchem-2064	225	59	)	)	PUNCT
eurjchem-2064	225	60	1181.4(3	1181.4(3	NOUN
eurjchem-2064	225	61	)	)	PUNCT
eurjchem-2064	225	62	1182.27(2	1182.27(2	NUM
eurjchem-2064	225	63	)	)	PUNCT
eurjchem-2064	225	64	1253.38(3	1253.38(3	NUM
eurjchem-2064	225	65	)	)	PUNCT
eurjchem-2064	225	66	crystal	crystal	NOUN
eurjchem-2064	225	67	size	size	NOUN
eurjchem-2064	225	68	(	(	PUNCT
eurjchem-2064	225	69	mm	mm	NOUN
eurjchem-2064	225	70	)	)	PUNCT
eurjchem-2064	225	71	0.354	0.354	NUM
eurjchem-2064	225	72	×	×	NOUN
eurjchem-2064	225	73	0.232	0.232	NUM
eurjchem-2064	225	74	×	×	NOUN
eurjchem-2064	225	75	0.188	0.188	NUM
eurjchem-2064	225	76	0.275	0.275	NUM
eurjchem-2064	225	77	×	×	NOUN
eurjchem-2064	225	78	0.164	0.164	NUM
eurjchem-2064	225	79	×	×	NOUN
eurjchem-2064	225	80	0.118	0.118	NUM
eurjchem-2064	225	81	0.478	0.478	NUM
eurjchem-2064	225	82	×	×	NOUN
eurjchem-2064	225	83	0.293	0.293	NUM
eurjchem-2064	225	84	×	×	NOUN
eurjchem-2064	225	85	0.15	0.15	NUM
eurjchem-2064	225	86	0.431	0.431	NUM
eurjchem-2064	225	87	×	×	NOUN
eurjchem-2064	225	88	0.425	0.425	NUM
eurjchem-2064	225	89	×	×	NOUN
eurjchem-2064	225	90	0.322	0.322	NUM
eurjchem-2064	225	91	radiation	radiation	NOUN
eurjchem-2064	225	92	type	type	NOUN
eurjchem-2064	225	93	cu	cu	PROPN
eurjchem-2064	225	94	kα	kα	PROPN
eurjchem-2064	225	95	mo	mo	PROPN
eurjchem-2064	225	96	kα	kα	PROPN
eurjchem-2064	225	97	cu	cu	PROPN
eurjchem-2064	226	1	kα	kα	PROPN
eurjchem-2064	226	2	cu	cu	PROPN
eurjchem-2064	226	3	kα	kα	PROPN
eurjchem-2064	226	4	t	t	PROPN
eurjchem-2064	226	5	(	(	PUNCT
eurjchem-2064	226	6	k	k	NOUN
eurjchem-2064	226	7	)	)	PUNCT
eurjchem-2064	226	8	173	173	NUM
eurjchem-2064	227	1	k	k	NOUN
eurjchem-2064	227	2	173	173	NUM
eurjchem-2064	228	1	k	k	NOUN
eurjchem-2064	228	2	173	173	NUM
eurjchem-2064	229	1	k	k	NOUN
eurjchem-2064	229	2	173	173	NUM
eurjchem-2064	229	3	k	k	PROPN
eurjchem-2064	229	4	μ	μ	PROPN
eurjchem-2064	229	5	(	(	PUNCT
eurjchem-2064	229	6	mm-1	mm-1	NOUN
eurjchem-2064	229	7	)	)	PUNCT
eurjchem-2064	229	8	2.015	2.015	NUM
eurjchem-2064	229	9	0.266	0.266	NUM
eurjchem-2064	229	10	2.284	2.284	NUM
eurjchem-2064	229	11	2.211	2.211	NUM
eurjchem-2064	229	12	dx	dx	PROPN
eurjchem-2064	229	13	(	(	PUNCT
eurjchem-2064	229	14	mg	mg	PROPN
eurjchem-2064	229	15	m-3	m-3	NUM
eurjchem-2064	229	16	)	)	PUNCT
eurjchem-2064	229	17	1.296	1.296	NUM
eurjchem-2064	229	18	1.357	1.357	NUM
eurjchem-2064	229	19	1.277	1.277	NUM
eurjchem-2064	229	20	1.311	1.311	NUM
eurjchem-2064	229	21	z	z	NOUN
eurjchem-2064	229	22	4	4	NUM
eurjchem-2064	229	23	4	4	NUM
eurjchem-2064	229	24	4	4	NUM
eurjchem-2064	229	25	4	4	NUM
eurjchem-2064	229	26	data	datum	NOUN
eurjchem-2064	229	27	collection	collection	NOUN
eurjchem-2064	229	28	tmin	tmin	NOUN
eurjchem-2064	229	29	0.663	0.663	NUM
eurjchem-2064	229	30	0.688	0.688	NUM
eurjchem-2064	229	31	0.658	0.658	NUM
eurjchem-2064	229	32	0.647	0.647	NUM
eurjchem-2064	229	33	tmax	tmax	ADP
eurjchem-2064	229	34	0.753	0.753	NUM
eurjchem-2064	229	35	0.745	0.745	NUM
eurjchem-2064	229	36	0.754	0.754	NUM
eurjchem-2064	229	37	0.754	0.754	NUM
eurjchem-2064	229	38	measured	measure	VERB
eurjchem-2064	229	39	reflections	reflection	NOUN
eurjchem-2064	229	40	12252	12252	NUM
eurjchem-2064	229	41	9976	9976	NUM
eurjchem-2064	229	42	13296	13296	NUM
eurjchem-2064	229	43	19721	19721	NUM
eurjchem-2064	229	44	independent	independent	ADJ
eurjchem-2064	229	45	reflections	reflection	NOUN
eurjchem-2064	229	46	2631	2631	NUM
eurjchem-2064	229	47	2330	2330	NUM
eurjchem-2064	229	48	2324	2324	NUM
eurjchem-2064	229	49	2457	2457	NUM
eurjchem-2064	229	50	reflections	reflection	NOUN
eurjchem-2064	229	51	with	with	ADP
eurjchem-2064	229	52	i	i	PRON
eurjchem-2064	229	53	>	>	X
eurjchem-2064	229	54	2σ(i	2σ(i	NUM
eurjchem-2064	229	55	)	)	PUNCT
eurjchem-2064	229	56	2219	2219	NUM
eurjchem-2064	229	57	1829	1829	NUM
eurjchem-2064	229	58	2104	2104	NUM
eurjchem-2064	229	59	2380	2380	NUM
eurjchem-2064	229	60	rint	rint	NOUN
eurjchem-2064	229	61	0.038	0.038	NUM
eurjchem-2064	229	62	0.038	0.038	NUM
eurjchem-2064	229	63	0.029	0.029	NUM
eurjchem-2064	229	64	0.032	0.032	NUM
eurjchem-2064	229	65	θmax	θmax	NOUN
eurjchem-2064	229	66	(	(	PUNCT
eurjchem-2064	229	67	°	°	PROPN
eurjchem-2064	229	68	)	)	PUNCT
eurjchem-2064	229	69	70.2	70.2	NUM
eurjchem-2064	229	70	26.1	26.1	NUM
eurjchem-2064	229	71	72.1	72.1	NUM
eurjchem-2064	229	72	72.1	72.1	NUM
eurjchem-2064	229	73	θmin	θmin	NOUN
eurjchem-2064	229	74	(	(	PUNCT
eurjchem-2064	229	75	°	°	PROPN
eurjchem-2064	229	76	)	)	PUNCT
eurjchem-2064	229	77	3.1	3.1	NUM
eurjchem-2064	229	78	2.3	2.3	NUM
eurjchem-2064	229	79	5.4	5.4	NUM
eurjchem-2064	229	80	5.4	5.4	NUM
eurjchem-2064	229	81	refinement	refinement	NOUN
eurjchem-2064	229	82	reflections	reflection	NOUN
eurjchem-2064	229	83	2631	2631	NUM
eurjchem-2064	229	84	2330	2330	NUM
eurjchem-2064	229	85	2324	2324	NUM
eurjchem-2064	229	86	2457	2457	NUM
eurjchem-2064	229	87	parameters	parameter	NOUN
eurjchem-2064	229	88	174	174	NUM
eurjchem-2064	229	89	146	146	NUM
eurjchem-2064	229	90	142	142	NUM
eurjchem-2064	229	91	159	159	NUM
eurjchem-2064	229	92	wr(f2	wr(f2	NOUN
eurjchem-2064	229	93	)	)	PUNCT
eurjchem-2064	229	94	0.120	0.120	NUM
eurjchem-2064	229	95	0.127	0.127	NUM
eurjchem-2064	229	96	0.104	0.104	NUM
eurjchem-2064	229	97	0.099	0.099	NUM
eurjchem-2064	229	98	r[f2	r[f2	NOUN
eurjchem-2064	229	99	>	>	X
eurjchem-2064	229	100	2σ(f2	2σ(f2	NUM
eurjchem-2064	229	101	)	)	PUNCT
eurjchem-2064	229	102	]	]	PUNCT
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eurjchem-2064	229	104	0.045	0.045	NUM
eurjchem-2064	229	105	0.037	0.037	NUM
eurjchem-2064	229	106	0.037	0.037	NUM
eurjchem-2064	229	107	s	s	PART
eurjchem-2064	229	108	1.04	1.04	NUM
eurjchem-2064	229	109	1.02	1.02	NUM
eurjchem-2064	229	110	1.05	1.05	NUM
eurjchem-2064	229	111	1.08	1.08	NUM
eurjchem-2064	229	112	δρmax	δρmax	NOUN
eurjchem-2064	229	113	(	(	PUNCT
eurjchem-2064	229	114	e	e	NOUN
eurjchem-2064	229	115	å-3	å-3	NUM
eurjchem-2064	229	116	)	)	PUNCT
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eurjchem-2064	229	118	0.31	0.31	NUM
eurjchem-2064	229	119	0.24	0.24	NUM
eurjchem-2064	229	120	0.21	0.21	NUM
eurjchem-2064	229	121	δρmin	δρmin	NOUN
eurjchem-2064	229	122	(	(	PUNCT
eurjchem-2064	229	123	e	e	NOUN
eurjchem-2064	229	124	å-3	å-3	NUM
eurjchem-2064	229	125	)	)	PUNCT
eurjchem-2064	230	1	−0.40	−0.40	X
eurjchem-2064	231	1	−0.29	−0.29	X
eurjchem-2064	232	1	−0.49	−0.49	X
eurjchem-2064	232	2	−0.47	−0.47	AUX
eurjchem-2064	232	3	compound	compound	VERB
eurjchem-2064	232	4	5	5	NUM
eurjchem-2064	232	5	11	11	NUM
eurjchem-2064	232	6	12	12	NUM
eurjchem-2064	232	7	molecular	molecular	ADJ
eurjchem-2064	232	8	formula	formula	NOUN
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eurjchem-2064	232	10	c11h15no4s	c11h15no4s	PROPN
eurjchem-2064	232	11	c15h25no2s	c15h25no2s	PROPN
eurjchem-2064	232	12	crystal	crystal	NOUN
eurjchem-2064	232	13	system	system	NOUN
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eurjchem-2064	232	15	orthorhombic	orthorhombic	NOUN
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eurjchem-2064	232	17	space	space	NOUN
eurjchem-2064	232	18	group	group	NOUN
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eurjchem-2064	233	5	a	a	DET
eurjchem-2064	233	6	(	(	PUNCT
eurjchem-2064	233	7	å	å	NOUN
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eurjchem-2064	233	12	)	)	PUNCT
eurjchem-2064	233	13	8.4584(15	8.4584(15	NUM
eurjchem-2064	233	14	)	)	PUNCT
eurjchem-2064	233	15	b	b	NOUN
eurjchem-2064	233	16	(	(	PUNCT
eurjchem-2064	233	17	å	å	NOUN
eurjchem-2064	233	18	)	)	PUNCT
eurjchem-2064	233	19	12.13534(18	12.13534(18	NUM
eurjchem-2064	233	20	)	)	PUNCT
eurjchem-2064	233	21	7.1268(6	7.1268(6	NOUN
eurjchem-2064	233	22	)	)	PUNCT
eurjchem-2064	233	23	8.7842(16	8.7842(16	NUM
eurjchem-2064	233	24	)	)	PUNCT
eurjchem-2064	233	25	c	c	NOUN
eurjchem-2064	233	26	(	(	PUNCT
eurjchem-2064	233	27	å	å	NOUN
eurjchem-2064	233	28	)	)	PUNCT
eurjchem-2064	233	29	16.3142(2	16.3142(2	NUM
eurjchem-2064	233	30	)	)	PUNCT
eurjchem-2064	233	31	19.8012(17	19.8012(17	NUM
eurjchem-2064	233	32	)	)	PUNCT
eurjchem-2064	233	33	11.251(2	11.251(2	NUM
eurjchem-2064	233	34	)	)	PUNCT
eurjchem-2064	233	35	α	α	PROPN
eurjchem-2064	233	36	(	(	PUNCT
eurjchem-2064	233	37	°	°	PROPN
eurjchem-2064	233	38	)	)	PUNCT
eurjchem-2064	233	39	90	90	NUM
eurjchem-2064	233	40	90	90	NUM
eurjchem-2064	233	41	98.6996(18	98.6996(18	NUM
eurjchem-2064	233	42	)	)	PUNCT
eurjchem-2064	233	43	β	β	X
eurjchem-2064	233	44	(	(	PUNCT
eurjchem-2064	233	45	°	°	PROPN
eurjchem-2064	233	46	)	)	PUNCT
eurjchem-2064	233	47	90	90	NUM
eurjchem-2064	233	48	90	90	NUM
eurjchem-2064	233	49	102.7748(18	102.7748(18	NUM
eurjchem-2064	233	50	)	)	PUNCT
eurjchem-2064	233	51	γ	γ	PROPN
eurjchem-2064	233	52	(	(	PUNCT
eurjchem-2064	233	53	°	°	PROPN
eurjchem-2064	233	54	)	)	PUNCT
eurjchem-2064	233	55	90	90	NUM
eurjchem-2064	233	56	90	90	NUM
eurjchem-2064	233	57	103.0230(18	103.0230(18	NUM
eurjchem-2064	233	58	)	)	PUNCT
eurjchem-2064	233	59	volume	volume	NOUN
eurjchem-2064	233	60	(	(	PUNCT
eurjchem-2064	233	61	å3	å3	PROPN
eurjchem-2064	233	62	)	)	PUNCT
eurjchem-2064	233	63	1218.72(3	1218.72(3	NUM
eurjchem-2064	233	64	)	)	PUNCT
eurjchem-2064	233	65	2520.0(4	2520.0(4	NOUN
eurjchem-2064	233	66	)	)	PUNCT
eurjchem-2064	233	67	776.3(2	776.3(2	NUM
eurjchem-2064	233	68	)	)	PUNCT
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eurjchem-2064	233	70	size	size	NOUN
eurjchem-2064	233	71	(	(	PUNCT
eurjchem-2064	233	72	mm	mm	NOUN
eurjchem-2064	233	73	)	)	PUNCT
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eurjchem-2064	233	75	×	×	NOUN
eurjchem-2064	233	76	0.247	0.247	NUM
eurjchem-2064	233	77	×	×	NOUN
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eurjchem-2064	233	79	0.31	0.31	NUM
eurjchem-2064	233	80	×	×	NOUN
eurjchem-2064	233	81	0.281	0.281	NUM
eurjchem-2064	233	82	×	×	NOUN
eurjchem-2064	233	83	0.172	0.172	NUM
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eurjchem-2064	233	85	×	×	NOUN
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eurjchem-2064	233	87	×	×	NOUN
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eurjchem-2064	233	90	type	type	NOUN
eurjchem-2064	234	1	cu	cu	PROPN
eurjchem-2064	235	1	kα	kα	PROPN
eurjchem-2064	236	1	mo	mo	PROPN
eurjchem-2064	237	1	kα	kα	PROPN
eurjchem-2064	238	1	mo	mo	PROPN
eurjchem-2064	239	1	kα	kα	PROPN
eurjchem-2064	240	1	t	t	PROPN
eurjchem-2064	241	1	(	(	PUNCT
eurjchem-2064	241	2	k	k	X
eurjchem-2064	241	3	)	)	PUNCT
eurjchem-2064	241	4	173	173	NUM
eurjchem-2064	241	5	173	173	NUM
eurjchem-2064	241	6	173	173	NUM
eurjchem-2064	241	7	μ	μ	NOUN
eurjchem-2064	241	8	(	(	PUNCT
eurjchem-2064	241	9	mm-1	mm-1	NOUN
eurjchem-2064	241	10	)	)	PUNCT
eurjchem-2064	241	11	2.246	2.246	NUM
eurjchem-2064	241	12	0.260	0.260	NUM
eurjchem-2064	241	13	0.207	0.207	NUM
eurjchem-2064	241	14	dx	dx	PROPN
eurjchem-2064	241	15	(	(	PUNCT
eurjchem-2064	241	16	mg	mg	PROPN
eurjchem-2064	241	17	m-3	m-3	PROPN
eurjchem-2064	241	18	)	)	PUNCT
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eurjchem-2064	242	2	1.367	1.367	NUM
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eurjchem-2064	242	4	z	z	NOUN
eurjchem-2064	242	5	4	4	NUM
eurjchem-2064	242	6	8	8	NUM
eurjchem-2064	242	7	2	2	NUM
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eurjchem-2064	242	9	collection	collection	NOUN
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eurjchem-2064	242	12	0.683	0.683	NUM
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eurjchem-2064	242	14	tmax	tmax	ADP
eurjchem-2064	242	15	0.754	0.754	NUM
eurjchem-2064	242	16	0.745	0.745	NUM
eurjchem-2064	242	17	0.745	0.745	NUM
eurjchem-2064	242	18	measured	measure	VERB
eurjchem-2064	242	19	reflections	reflection	NOUN
eurjchem-2064	242	20	11732	11732	NUM
eurjchem-2064	242	21	18825	18825	NUM
eurjchem-2064	242	22	13646	13646	NUM
eurjchem-2064	242	23	independent	independent	ADJ
eurjchem-2064	242	24	reflections	reflection	NOUN
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eurjchem-2064	242	26	2307	2307	NUM
eurjchem-2064	242	27	3166	3166	NUM
eurjchem-2064	242	28	reflections	reflection	NOUN
eurjchem-2064	242	29	with	with	ADP
eurjchem-2064	242	30	i	i	PRON
eurjchem-2064	242	31	>	>	X
eurjchem-2064	242	32	2σ(i	2σ(i	NUM
eurjchem-2064	242	33	)	)	PUNCT
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eurjchem-2064	242	35	1942	1942	NUM
eurjchem-2064	242	36	2692	2692	NUM
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eurjchem-2064	242	38	0.027	0.027	NUM
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eurjchem-2064	242	40	0.030	0.030	NUM
eurjchem-2064	242	41	θmax	θmax	NOUN
eurjchem-2064	242	42	(	(	PUNCT
eurjchem-2064	242	43	°	°	PROPN
eurjchem-2064	242	44	)	)	PUNCT
eurjchem-2064	242	45	72.1	72.1	NUM
eurjchem-2064	242	46	25.4	25.4	NUM
eurjchem-2064	242	47	26.4	26.4	NUM
eurjchem-2064	242	48	θmin	θmin	NOUN
eurjchem-2064	242	49	(	(	PUNCT
eurjchem-2064	242	50	°	°	PROPN
eurjchem-2064	242	51	)	)	PUNCT
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eurjchem-2064	242	53	2.1	2.1	NUM
eurjchem-2064	242	54	1.9	1.9	NUM
eurjchem-2064	242	55	refinement	refinement	NOUN
eurjchem-2064	242	56	reflections	reflection	NOUN
eurjchem-2064	242	57	2411	2411	NUM
eurjchem-2064	242	58	1942	1942	NUM
eurjchem-2064	242	59	2692	2692	NUM
eurjchem-2064	242	60	parameters	parameter	NOUN
eurjchem-2064	242	61	146	146	NUM
eurjchem-2064	242	62	163	163	NUM
eurjchem-2064	242	63	182	182	NUM
eurjchem-2064	242	64	wr(f2	wr(f2	NOUN
eurjchem-2064	242	65	)	)	PUNCT
eurjchem-2064	242	66	0.0931	0.0931	NUM
eurjchem-2064	243	1	0.1380	0.1380	NUM
eurjchem-2064	243	2	0.1106	0.1106	NUM
eurjchem-2064	243	3	r[f2	r[f2	NOUN
eurjchem-2064	243	4	>	>	X
eurjchem-2064	243	5	2σ(f2	2σ(f2	NUM
eurjchem-2064	243	6	)	)	PUNCT
eurjchem-2064	243	7	]	]	PUNCT
eurjchem-2064	244	1	0.0352	0.0352	NUM
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eurjchem-2064	244	4	s	s	PART
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eurjchem-2064	244	7	1.07	1.07	NUM
eurjchem-2064	244	8	δρmax	δρmax	NOUN
eurjchem-2064	244	9	(	(	PUNCT
eurjchem-2064	244	10	e	e	PROPN
eurjchem-2064	244	11	a	a	DET
eurjchem-2064	244	12	�	�	PROPN
eurjchem-2064	244	13	-3	-3	PUNCT
eurjchem-2064	244	14	)	)	PUNCT
eurjchem-2064	244	15	0.17	0.17	NUM
eurjchem-2064	244	16	0.64	0.64	NUM
eurjchem-2064	244	17	0.27	0.27	NUM
eurjchem-2064	244	18	δρmin	δρmin	NOUN
eurjchem-2064	244	19	(	(	PUNCT
eurjchem-2064	244	20	e	e	X
eurjchem-2064	244	21	a	a	DET
eurjchem-2064	244	22	�	�	PROPN
eurjchem-2064	244	23	-3	-3	PUNCT
eurjchem-2064	244	24	)	)	PUNCT
eurjchem-2064	245	1	−0.46	−0.46	PROPN
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eurjchem-2064	246	2	−0.39	−0.39	NOUN
eurjchem-2064	246	3	a	a	DET
eurjchem-2064	246	4	comparison	comparison	NOUN
eurjchem-2064	246	5	of	of	ADP
eurjchem-2064	246	6	the	the	DET
eurjchem-2064	246	7	resulting	result	VERB
eurjchem-2064	246	8	parameters	parameter	NOUN
eurjchem-2064	246	9	can	can	AUX
eurjchem-2064	246	10	be	be	AUX
eurjchem-2064	246	11	found	find	VERB
eurjchem-2064	246	12	in	in	ADP
eurjchem-2064	246	13	table	table	NOUN
eurjchem-2064	246	14	3	3	NUM
eurjchem-2064	246	15	.	.	PUNCT
eurjchem-2064	247	1	in	in	ADP
eurjchem-2064	247	2	addition	addition	NOUN
eurjchem-2064	247	3	to	to	ADP
eurjchem-2064	247	4	those	those	PRON
eurjchem-2064	247	5	mentioned	mention	VERB
eurjchem-2064	247	6	below	below	ADV
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eurjchem-2064	247	11	1-[(4	1-[(4	NOUN
eurjchem-2064	247	12	-	-	PUNCT
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eurjchem-2064	247	14	(	(	PUNCT
eurjchem-2064	247	15	3	3	NUM
eurjchem-2064	247	16	)	)	PUNCT
eurjchem-2064	247	17	,	,	PUNCT
eurjchem-2064	247	18	4	4	NUM
eurjchem-2064	247	19	-	-	PUNCT
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eurjchem-2064	247	21	-	-	PUNCT
eurjchem-2064	247	22	n-(4met	n-(4met	VERB
eurjchem-2064	247	23	-	-	PUNCT
eurjchem-2064	247	24	hylbenzyl)benzenesulfonamide	hylbenzyl)benzenesulfonamide	NOUN
eurjchem-2064	247	25	(	(	PUNCT
eurjchem-2064	247	26	8)	8)	NUM
eurjchem-2064	247	27	,	,	PUNCT
eurjchem-2064	247	28	and	and	CCONJ
eurjchem-2064	247	29	4	4	NUM
eurjchem-2064	247	30	-	-	PUNCT
eurjchem-2064	247	31	methyl	methyl	NOUN
eurjchem-2064	247	32	-	-	PUNCT
eurjchem-2064	247	33	n	n	CCONJ
eurjchem-2064	247	34	-	-	PUNCT
eurjchem-2064	247	35	propylbenzenesulfonamide	propylbenzenesulfonamide	NOUN
eurjchem-2064	247	36	(	(	PUNCT
eurjchem-2064	247	37	10	10	NUM
eurjchem-2064	247	38	)	)	PUNCT
eurjchem-2064	247	39	were	be	AUX
eurjchem-2064	247	40	previously	previously	ADV
eurjchem-2064	247	41	reported	report	VERB
eurjchem-2064	247	42	using	use	VERB
eurjchem-2064	247	43	the	the	DET
eurjchem-2064	247	44	conditions	condition	NOUN
eurjchem-2064	247	45	aforementioned	aforementione	VERB
eurjchem-2064	247	46	[	[	PUNCT
eurjchem-2064	247	47	29	29	NUM
eurjchem-2064	247	48	-	-	SYM
eurjchem-2064	247	49	31	31	NUM
eurjchem-2064	247	50	]	]	PUNCT
eurjchem-2064	247	51	.	.	PUNCT
eurjchem-2064	248	1	the	the	DET
eurjchem-2064	248	2	structures	structure	NOUN
eurjchem-2064	248	3	of	of	ADP
eurjchem-2064	248	4	4-[(4	4-[(4	NOUN
eurjchem-2064	248	5	-	-	PUNCT
eurjchem-2064	248	6	methylbenzene)sulfonyl	methylbenzene)sulfonyl	NOUN
eurjchem-2064	248	7	]	]	X
eurjchem-2064	248	8	morpholine	morpholine	NOUN
eurjchem-2064	248	9	(	(	PUNCT
eurjchem-2064	248	10	2	2	NUM
eurjchem-2064	248	11	)	)	PUNCT
eurjchem-2064	248	12	,	,	PUNCT
eurjchem-2064	248	13	4	4	NUM
eurjchem-2064	248	14	-	-	PUNCT
eurjchem-2064	248	15	methyl	methyl	NOUN
eurjchem-2064	248	16	-	-	PUNCT
eurjchem-2064	248	17	n	n	CCONJ
eurjchem-2064	248	18	-	-	PUNCT
eurjchem-2064	248	19	phenylbenzenesulfonamide	phenylbenzenesulfonamide	NOUN
eurjchem-2064	248	20	(	(	PUNCT
eurjchem-2064	248	21	9	9	NUM
eurjchem-2064	248	22	)	)	PUNCT
eurjchem-2064	248	23	,	,	PUNCT
eurjchem-2064	248	24	n	n	CCONJ
eurjchem-2064	248	25	-	-	PUNCT
eurjchem-2064	248	26	benzyln,4	benzyln,4	NOUN
eurjchem-2064	248	27	-	-	PUNCT
eurjchem-2064	248	28	dimethylbenzenesulfonamide	dimethylbenzenesulfonamide	NOUN
eurjchem-2064	248	29	(	(	PUNCT
eurjchem-2064	248	30	1	1	NUM
eurjchem-2064	248	31	)	)	PUNCT
eurjchem-2064	248	32	,	,	PUNCT
eurjchem-2064	248	33	and	and	CCONJ
eurjchem-2064	248	34	n	n	CCONJ
eurjchem-2064	248	35	-	-	PUNCT
eurjchem-2064	248	36	butyl-4	butyl-4	NOUN
eurjchem-2064	248	37	-	-	PUNCT
eurjchem-2064	248	38	methyl	methyl	NOUN
eurjchem-2064	248	39	benzenesulfonamide	benzenesulfonamide	NOUN
eurjchem-2064	248	40	(	(	PUNCT
eurjchem-2064	248	41	4	4	X
eurjchem-2064	248	42	)	)	PUNCT
eurjchem-2064	248	43	exhibited	exhibit	VERB
eurjchem-2064	248	44	monoclinic	monoclinic	ADJ
eurjchem-2064	248	45	systems	system	NOUN
eurjchem-2064	248	46	(	(	PUNCT
eurjchem-2064	248	47	p21	p21	NOUN
eurjchem-2064	248	48	/	/	SYM
eurjchem-2064	248	49	c	c	NOUN
eurjchem-2064	248	50	space	space	NOUN
eurjchem-2064	248	51	group	group	NOUN
eurjchem-2064	248	52	)	)	PUNCT
eurjchem-2064	248	53	both	both	CCONJ
eurjchem-2064	248	54	with	with	ADP
eurjchem-2064	248	55	one	one	NUM
eurjchem-2064	248	56	screw	screw	NOUN
eurjchem-2064	248	57	axis	axis	NOUN
eurjchem-2064	248	58	(	(	PUNCT
eurjchem-2064	248	59	2	2	NUM
eurjchem-2064	248	60	-	-	NOUN
eurjchem-2064	248	61	fold	fold	ADJ
eurjchem-2064	248	62	)	)	PUNCT
eurjchem-2064	248	63	and	and	CCONJ
eurjchem-2064	248	64	one	one	NUM
eurjchem-2064	248	65	glide	glide	ADJ
eurjchem-2064	248	66	plane	plane	NOUN
eurjchem-2064	248	67	geometry	geometry	NOUN
eurjchem-2064	248	68	and	and	CCONJ
eurjchem-2064	248	69	an	an	DET
eurjchem-2064	248	70	inversion	inversion	NOUN
eurjchem-2064	248	71	center	center	NOUN
eurjchem-2064	248	72	.	.	PUNCT
eurjchem-2064	249	1	1-[(4	1-[(4	ADJ
eurjchem-2064	249	2	-	-	PUNCT
eurjchem-2064	249	3	methylbenzene	methylbenzene	NOUN
eurjchem-2064	249	4	)	)	PUNCT
eurjchem-2064	249	5	sulfonyl]piperidine	sulfonyl]piperidine	PROPN
eurjchem-2064	249	6	(	(	PUNCT
eurjchem-2064	249	7	5	5	NUM
eurjchem-2064	249	8	)	)	PUNCT
eurjchem-2064	249	9	showed	show	VERB
eurjchem-2064	249	10	an	an	DET
eurjchem-2064	249	11	orthorhombic	orthorhombic	NOUN
eurjchem-2064	249	12	system	system	NOUN
eurjchem-2064	249	13	(	(	PUNCT
eurjchem-2064	249	14	p212121	p212121	ADJ
eurjchem-2064	249	15	space	space	NOUN
eurjchem-2064	249	16	group	group	NOUN
eurjchem-2064	249	17	)	)	PUNCT
eurjchem-2064	249	18	and	and	CCONJ
eurjchem-2064	249	19	had	have	VERB
eurjchem-2064	249	20	both	both	DET
eurjchem-2064	249	21	one	one	NUM
eurjchem-2064	249	22	screw	screw	VERB
eurjchem-2064	249	23	axis	axis	NOUN
eurjchem-2064	249	24	(	(	PUNCT
eurjchem-2064	249	25	2	2	NUM
eurjchem-2064	249	26	-	-	NOUN
eurjchem-2064	249	27	fold	fold	ADJ
eurjchem-2064	249	28	)	)	PUNCT
eurjchem-2064	249	29	and	and	CCONJ
eurjchem-2064	249	30	one	one	NUM
eurjchem-2064	249	31	glide	glide	ADJ
eurjchem-2064	249	32	plane	plane	NOUN
eurjchem-2064	249	33	geometry	geometry	NOUN
eurjchem-2064	249	34	but	but	CCONJ
eurjchem-2064	249	35	lacked	lack	VERB
eurjchem-2064	249	36	an	an	DET
eurjchem-2064	249	37	inversion	inversion	NOUN
eurjchem-2064	249	38	center	center	NOUN
eurjchem-2064	249	39	.	.	PUNCT
eurjchem-2064	250	1	4methyl	4methyl	PROPN
eurjchem-2064	250	2	-	-	PUNCT
eurjchem-2064	250	3	n-(2	n-(2	PROPN
eurjchem-2064	250	4	,	,	PUNCT
eurjchem-2064	250	5	4	4	NUM
eurjchem-2064	250	6	,	,	PUNCT
eurjchem-2064	250	7	4	4	NUM
eurjchem-2064	250	8	-	-	PUNCT
eurjchem-2064	250	9	trimethylpentan-2	trimethylpentan-2	NOUN
eurjchem-2064	250	10	-	-	PUNCT
eurjchem-2064	250	11	yl	yl	NOUN
eurjchem-2064	250	12	)	)	PUNCT
eurjchem-2064	250	13	benzenesulfonamide	benzenesulfonamide	NOUN
eurjchem-2064	250	14	(	(	PUNCT
eurjchem-2064	250	15	12	12	NUM
eurjchem-2064	250	16	)	)	PUNCT
eurjchem-2064	250	17	revealed	reveal	VERB
eurjchem-2064	250	18	a	a	DET
eurjchem-2064	250	19	triclinic	triclinic	ADJ
eurjchem-2064	250	20	system	system	NOUN
eurjchem-2064	250	21	(	(	PUNCT
eurjchem-2064	250	22	p-1	p-1	NOUN
eurjchem-2064	250	23	space	space	NOUN
eurjchem-2064	250	24	group	group	NOUN
eurjchem-2064	250	25	)	)	PUNCT
eurjchem-2064	250	26	with	with	ADP
eurjchem-2064	250	27	only	only	ADV
eurjchem-2064	250	28	an	an	DET
eurjchem-2064	250	29	inversion	inversion	NOUN
eurjchem-2064	250	30	center	center	NOUN
eurjchem-2064	250	31	.	.	PUNCT
eurjchem-2064	251	1	stenfors	stenfor	NOUN
eurjchem-2064	251	2	and	and	CCONJ
eurjchem-2064	251	3	ngassa	ngassa	NOUN
eurjchem-2064	251	4	/	/	SYM
eurjchem-2064	251	5	european	european	ADJ
eurjchem-2064	251	6	journal	journal	PROPN
eurjchem-2064	251	7	of	of	ADP
eurjchem-2064	251	8	chemistry	chemistry	NOUN
eurjchem-2064	251	9	12	12	NUM
eurjchem-2064	251	10	(	(	PUNCT
eurjchem-2064	251	11	2	2	NUM
eurjchem-2064	251	12	)	)	PUNCT
eurjchem-2064	251	13	(	(	PUNCT
eurjchem-2064	251	14	2021	2021	NUM
eurjchem-2064	251	15	)	)	PUNCT
eurjchem-2064	251	16	109	109	NUM
eurjchem-2064	251	17	-	-	SYM
eurjchem-2064	251	18	116	116	NUM
eurjchem-2064	251	19	115	115	NUM
eurjchem-2064	251	20	2021	2021	NUM
eurjchem-2064	251	21	–	–	PUNCT
eurjchem-2064	251	22	european	european	ADJ
eurjchem-2064	251	23	journal	journal	NOUN
eurjchem-2064	251	24	of	of	ADP
eurjchem-2064	251	25	chemistry	chemistry	NOUN
eurjchem-2064	251	26	–	–	PUNCT
eurjchem-2064	251	27	cc	cc	NOUN
eurjchem-2064	251	28	by	by	ADP
eurjchem-2064	251	29	nc	nc	PROPN
eurjchem-2064	251	30	–	–	PUNCT
eurjchem-2064	251	31	doi	doi	NOUN
eurjchem-2064	251	32	:	:	PUNCT
eurjchem-2064	251	33	10.5155	10.5155	NUM
eurjchem-2064	251	34	/	/	SYM
eurjchem-2064	251	35	eurjchem.12.2.109	eurjchem.12.2.109	NUM
eurjchem-2064	251	36	-	-	PUNCT
eurjchem-2064	251	37	116.2064	116.2064	NUM
eurjchem-2064	251	38	table	table	NOUN
eurjchem-2064	251	39	4	4	NUM
eurjchem-2064	251	40	.	.	PUNCT
eurjchem-2064	251	41	c1	c1	NOUN
eurjchem-2064	251	42	-	-	PUNCT
eurjchem-2064	251	43	s1	s1	NOUN
eurjchem-2064	251	44	-	-	PUNCT
eurjchem-2064	251	45	n1	n1	NOUN
eurjchem-2064	251	46	-	-	PUNCT
eurjchem-2064	251	47	c	c	NOUN
eurjchem-2064	251	48	torsion	torsion	NOUN
eurjchem-2064	251	49	angles	angle	NOUN
eurjchem-2064	251	50	(	(	PUNCT
eurjchem-2064	251	51	°	°	NOUN
eurjchem-2064	251	52	)	)	PUNCT
eurjchem-2064	251	53	of	of	ADP
eurjchem-2064	251	54	sulfonamide	sulfonamide	NOUN
eurjchem-2064	251	55	crystal	crystal	NOUN
eurjchem-2064	251	56	structures	structure	NOUN
eurjchem-2064	251	57	.	.	PUNCT
eurjchem-2064	252	1	atoms	atom	NOUN
eurjchem-2064	252	2	numbering	numbering	NOUN
eurjchem-2064	252	3	follows	follow	VERB
eurjchem-2064	252	4	scheme	scheme	NOUN
eurjchem-2064	252	5	in	in	ADP
eurjchem-2064	252	6	figure	figure	NOUN
eurjchem-2064	252	7	3	3	NUM
eurjchem-2064	252	8	.	.	PUNCT
eurjchem-2064	253	1	compound	compound	NOUN
eurjchem-2064	253	2	torsion	torsion	NOUN
eurjchem-2064	253	3	angle	angle	NOUN
eurjchem-2064	253	4	(	(	PUNCT
eurjchem-2064	253	5	°	°	NOUN
eurjchem-2064	253	6	)	)	PUNCT
eurjchem-2064	253	7	n	n	CCONJ
eurjchem-2064	253	8	-	-	PUNCT
eurjchem-2064	253	9	benzyl	benzyl	NOUN
eurjchem-2064	253	10	-	-	PUNCT
eurjchem-2064	253	11	n,4	n,4	PRON
eurjchem-2064	253	12	-	-	PUNCT
eurjchem-2064	253	13	dimethylbenzenesulfonamide	dimethylbenzenesulfonamide	NOUN
eurjchem-2064	253	14	(	(	PUNCT
eurjchem-2064	253	15	1	1	X
eurjchem-2064	253	16	)	)	PUNCT
eurjchem-2064	253	17	c1	c1	NOUN
eurjchem-2064	253	18	-	-	PUNCT
eurjchem-2064	253	19	s1	s1	NOUN
eurjchem-2064	253	20	-	-	PUNCT
eurjchem-2064	253	21	n1	n1	NOUN
eurjchem-2064	253	22	-	-	PUNCT
eurjchem-2064	253	23	c8	c8	PROPN
eurjchem-2064	253	24	63.1(2	63.1(2	PROPN
eurjchem-2064	253	25	)	)	PUNCT
eurjchem-2064	253	26	c1	c1	NOUN
eurjchem-2064	253	27	-	-	PUNCT
eurjchem-2064	253	28	s1	s1	NOUN
eurjchem-2064	253	29	-	-	PUNCT
eurjchem-2064	253	30	n1	n1	NOUN
eurjchem-2064	253	31	-	-	PUNCT
eurjchem-2064	253	32	c9	c9	NOUN
eurjchem-2064	253	33	-71.6(2	-71.6(2	NOUN
eurjchem-2064	253	34	)	)	PUNCT
eurjchem-2064	253	35	4-[(4	4-[(4	NOUN
eurjchem-2064	253	36	-	-	PUNCT
eurjchem-2064	253	37	methylbenzene)sulfonyl]morpholine	methylbenzene)sulfonyl]morpholine	X
eurjchem-2064	253	38	(	(	PUNCT
eurjchem-2064	253	39	2	2	X
eurjchem-2064	253	40	)	)	PUNCT
eurjchem-2064	253	41	c1	c1	NOUN
eurjchem-2064	253	42	-	-	PUNCT
eurjchem-2064	253	43	s1	s1	NOUN
eurjchem-2064	253	44	-	-	PUNCT
eurjchem-2064	253	45	n1	n1	NOUN
eurjchem-2064	253	46	-	-	PUNCT
eurjchem-2064	253	47	c8	c8	PROPN
eurjchem-2064	253	48	-65.2(2	-65.2(2	PROPN
eurjchem-2064	253	49	)	)	PUNCT
eurjchem-2064	253	50	c1	c1	PROPN
eurjchem-2064	253	51	-	-	PUNCT
eurjchem-2064	253	52	s1	s1	NOUN
eurjchem-2064	253	53	-	-	PUNCT
eurjchem-2064	253	54	n1	n1	NOUN
eurjchem-2064	253	55	-	-	PUNCT
eurjchem-2064	253	56	c11	c11	NOUN
eurjchem-2064	253	57	68.8(2	68.8(2	NOUN
eurjchem-2064	253	58	)	)	PUNCT
eurjchem-2064	253	59	n	n	CCONJ
eurjchem-2064	253	60	-	-	PUNCT
eurjchem-2064	253	61	butyl-4	butyl-4	NOUN
eurjchem-2064	253	62	-	-	PUNCT
eurjchem-2064	253	63	methylbenzenesulfonamide	methylbenzenesulfonamide	NOUN
eurjchem-2064	253	64	(	(	PUNCT
eurjchem-2064	253	65	4	4	X
eurjchem-2064	253	66	)	)	PUNCT
eurjchem-2064	253	67	c1	c1	NOUN
eurjchem-2064	253	68	-	-	PUNCT
eurjchem-2064	253	69	s1	s1	NOUN
eurjchem-2064	253	70	-	-	PUNCT
eurjchem-2064	253	71	n1	n1	NOUN
eurjchem-2064	253	72	-	-	PUNCT
eurjchem-2064	253	73	c8	c8	NOUN
eurjchem-2064	253	74	-61.1(1	-61.1(1	ADJ
eurjchem-2064	253	75	)	)	PUNCT
eurjchem-2064	253	76	1-[(4	1-[(4	ADJ
eurjchem-2064	253	77	-	-	PUNCT
eurjchem-2064	253	78	methylbenzene)sulfonyl]piperidine	methylbenzene)sulfonyl]piperidine	NOUN
eurjchem-2064	253	79	(	(	PUNCT
eurjchem-2064	253	80	5	5	NUM
eurjchem-2064	253	81	)	)	PUNCT
eurjchem-2064	253	82	c1	c1	NOUN
eurjchem-2064	253	83	-	-	PUNCT
eurjchem-2064	253	84	s1	s1	NOUN
eurjchem-2064	253	85	-	-	PUNCT
eurjchem-2064	253	86	n1	n1	NOUN
eurjchem-2064	253	87	-	-	PUNCT
eurjchem-2064	253	88	c8	c8	NOUN
eurjchem-2064	253	89	67.8(1	67.8(1	PROPN
eurjchem-2064	253	90	)	)	PUNCT
eurjchem-2064	253	91	c1	c1	NOUN
eurjchem-2064	253	92	-	-	PUNCT
eurjchem-2064	253	93	s1	s1	NOUN
eurjchem-2064	253	94	-	-	PUNCT
eurjchem-2064	253	95	n1	n1	NOUN
eurjchem-2064	253	96	-	-	PUNCT
eurjchem-2064	253	97	c12	c12	NOUN
eurjchem-2064	253	98	-70.7(1	-70.7(1	PROPN
eurjchem-2064	253	99	)	)	PUNCT
eurjchem-2064	253	100	4	4	NUM
eurjchem-2064	253	101	-	-	PUNCT
eurjchem-2064	253	102	methyl	methyl	NOUN
eurjchem-2064	253	103	-	-	PUNCT
eurjchem-2064	253	104	n	n	CCONJ
eurjchem-2064	253	105	-	-	PUNCT
eurjchem-2064	253	106	phenylbenzenesulfonamide	phenylbenzenesulfonamide	NOUN
eurjchem-2064	253	107	(	(	PUNCT
eurjchem-2064	253	108	9	9	NUM
eurjchem-2064	253	109	)	)	PUNCT
eurjchem-2064	253	110	c1	c1	NOUN
eurjchem-2064	253	111	-	-	PUNCT
eurjchem-2064	253	112	s1	s1	NOUN
eurjchem-2064	253	113	-	-	PUNCT
eurjchem-2064	253	114	n1	n1	NOUN
eurjchem-2064	253	115	-	-	PUNCT
eurjchem-2064	253	116	c8	c8	NOUN
eurjchem-2064	253	117	-50.6(1	-50.6(1	PROPN
eurjchem-2064	253	118	)	)	PUNCT
eurjchem-2064	253	119	n	n	CCONJ
eurjchem-2064	253	120	,	,	PUNCT
eurjchem-2064	253	121	n	n	CCONJ
eurjchem-2064	253	122	-	-	PUNCT
eurjchem-2064	253	123	bis(2	bis(2	NOUN
eurjchem-2064	253	124	-	-	PUNCT
eurjchem-2064	253	125	hydroxyethyl)-4	hydroxyethyl)-4	NOUN
eurjchem-2064	253	126	-	-	PUNCT
eurjchem-2064	253	127	methylbenzenesulfonamide	methylbenzenesulfonamide	NOUN
eurjchem-2064	253	128	(	(	PUNCT
eurjchem-2064	253	129	11	11	NUM
eurjchem-2064	253	130	)	)	PUNCT
eurjchem-2064	253	131	c1	c1	NOUN
eurjchem-2064	253	132	-	-	PUNCT
eurjchem-2064	253	133	s1	s1	NOUN
eurjchem-2064	253	134	-	-	PUNCT
eurjchem-2064	253	135	n1	n1	NOUN
eurjchem-2064	253	136	-	-	PUNCT
eurjchem-2064	253	137	c8	c8	NOUN
eurjchem-2064	253	138	86.4(2	86.4(2	PROPN
eurjchem-2064	253	139	)	)	PUNCT
eurjchem-2064	253	140	c1	c1	NOUN
eurjchem-2064	253	141	-	-	PUNCT
eurjchem-2064	253	142	s1	s1	NOUN
eurjchem-2064	253	143	-	-	PUNCT
eurjchem-2064	253	144	n1	n1	NOUN
eurjchem-2064	253	145	-	-	PUNCT
eurjchem-2064	253	146	c10	c10	NOUN
eurjchem-2064	253	147	-62.9(2	-62.9(2	PROPN
eurjchem-2064	253	148	)	)	PUNCT
eurjchem-2064	253	149	4	4	NUM
eurjchem-2064	253	150	-	-	PUNCT
eurjchem-2064	253	151	methyl	methyl	NOUN
eurjchem-2064	253	152	-	-	PUNCT
eurjchem-2064	253	153	n-(2,4,4	n-(2,4,4	VERB
eurjchem-2064	253	154	-	-	PUNCT
eurjchem-2064	253	155	trimethylpentan-2	trimethylpentan-2	NOUN
eurjchem-2064	253	156	-	-	PUNCT
eurjchem-2064	253	157	yl)benzenesulfonamide	yl)benzenesulfonamide	NOUN
eurjchem-2064	253	158	(	(	PUNCT
eurjchem-2064	253	159	12	12	NUM
eurjchem-2064	253	160	)	)	PUNCT
eurjchem-2064	253	161	c1	c1	NOUN
eurjchem-2064	253	162	-	-	PUNCT
eurjchem-2064	253	163	s1	s1	NOUN
eurjchem-2064	253	164	-	-	PUNCT
eurjchem-2064	253	165	n1	n1	NOUN
eurjchem-2064	253	166	-	-	PUNCT
eurjchem-2064	253	167	c8	c8	NOUN
eurjchem-2064	253	168	78.3(2	78.3(2	PROPN
eurjchem-2064	253	169	)	)	PUNCT
eurjchem-2064	253	170	(	(	PUNCT
eurjchem-2064	253	171	a	a	NOUN
eurjchem-2064	253	172	)	)	PUNCT
eurjchem-2064	253	173	(	(	PUNCT
eurjchem-2064	253	174	b	b	X
eurjchem-2064	253	175	)	)	PUNCT
eurjchem-2064	253	176	figure	figure	NOUN
eurjchem-2064	253	177	5	5	NUM
eurjchem-2064	253	178	.	.	PUNCT
eurjchem-2064	253	179	depiction	depiction	NOUN
eurjchem-2064	253	180	of	of	ADP
eurjchem-2064	253	181	hydrogen	hydrogen	NOUN
eurjchem-2064	253	182	bond	bond	NOUN
eurjchem-2064	253	183	contacts	contact	NOUN
eurjchem-2064	253	184	(	(	PUNCT
eurjchem-2064	253	185	a	a	NOUN
eurjchem-2064	253	186	)	)	PUNCT
eurjchem-2064	253	187	and	and	CCONJ
eurjchem-2064	253	188	the	the	DET
eurjchem-2064	253	189	o3	o3	PROPN
eurjchem-2064	253	190	-	-	PUNCT
eurjchem-2064	253	191	h10a	h10a	PROPN
eurjchem-2064	253	192	hydrogen	hydrogen	NOUN
eurjchem-2064	253	193	bond	bond	NOUN
eurjchem-2064	253	194	contact	contact	NOUN
eurjchem-2064	253	195	(	(	PUNCT
eurjchem-2064	253	196	b	b	NOUN
eurjchem-2064	253	197	)	)	PUNCT
eurjchem-2064	253	198	present	present	NOUN
eurjchem-2064	253	199	in	in	ADP
eurjchem-2064	253	200	the	the	DET
eurjchem-2064	253	201	crystal	crystal	NOUN
eurjchem-2064	253	202	structure	structure	NOUN
eurjchem-2064	253	203	of	of	ADP
eurjchem-2064	253	204	4-[(4methylbenzene)sulfonyl]morpholine	4-[(4methylbenzene)sulfonyl]morpholine	NUM
eurjchem-2064	253	205	(	(	PUNCT
eurjchem-2064	253	206	2	2	NUM
eurjchem-2064	253	207	)	)	PUNCT
eurjchem-2064	253	208	.	.	PUNCT
eurjchem-2064	254	1	n	n	CCONJ
eurjchem-2064	254	2	,	,	PUNCT
eurjchem-2064	254	3	n	n	CCONJ
eurjchem-2064	254	4	-	-	PUNCT
eurjchem-2064	254	5	bis(2	bis(2	NOUN
eurjchem-2064	254	6	-	-	PUNCT
eurjchem-2064	254	7	hydroxyethyl)-4	hydroxyethyl)-4	VERB
eurjchem-2064	254	8	-	-	PUNCT
eurjchem-2064	254	9	methylbenzene	methylbenzene	NOUN
eurjchem-2064	254	10	sulfonamide	sulfonamide	NOUN
eurjchem-2064	254	11	(	(	PUNCT
eurjchem-2064	254	12	11	11	NUM
eurjchem-2064	254	13	)	)	PUNCT
eurjchem-2064	254	14	exhibited	exhibit	VERB
eurjchem-2064	254	15	an	an	DET
eurjchem-2064	254	16	orthorhombic	orthorhombic	NOUN
eurjchem-2064	254	17	system	system	NOUN
eurjchem-2064	254	18	(	(	PUNCT
eurjchem-2064	254	19	pbca	pbca	ADJ
eurjchem-2064	254	20	space	space	NOUN
eurjchem-2064	254	21	group	group	NOUN
eurjchem-2064	254	22	)	)	PUNCT
eurjchem-2064	254	23	with	with	ADP
eurjchem-2064	254	24	three	three	NUM
eurjchem-2064	254	25	-	-	PUNCT
eurjchem-2064	254	26	screw	screw	ADJ
eurjchem-2064	254	27	axis	axis	NOUN
eurjchem-2064	254	28	(	(	PUNCT
eurjchem-2064	254	29	2	2	NUM
eurjchem-2064	254	30	-	-	NOUN
eurjchem-2064	254	31	fold	fold	ADJ
eurjchem-2064	254	32	)	)	PUNCT
eurjchem-2064	254	33	and	and	CCONJ
eurjchem-2064	254	34	three	three	NUM
eurjchem-2064	254	35	glide	glide	ADJ
eurjchem-2064	254	36	plane	plane	NOUN
eurjchem-2064	254	37	geometries	geometry	NOUN
eurjchem-2064	254	38	as	as	ADV
eurjchem-2064	254	39	well	well	ADV
eurjchem-2064	254	40	as	as	ADP
eurjchem-2064	254	41	an	an	DET
eurjchem-2064	254	42	inversion	inversion	NOUN
eurjchem-2064	254	43	center	center	NOUN
eurjchem-2064	254	44	.	.	PUNCT
eurjchem-2064	255	1	all	all	DET
eurjchem-2064	255	2	structures	structure	NOUN
eurjchem-2064	255	3	were	be	AUX
eurjchem-2064	255	4	oriented	orient	VERB
eurjchem-2064	255	5	gauche	gauche	NOUN
eurjchem-2064	255	6	about	about	ADP
eurjchem-2064	255	7	the	the	DET
eurjchem-2064	255	8	s1	s1	NOUN
eurjchem-2064	255	9	-	-	PUNCT
eurjchem-2064	255	10	n1	n1	NOUN
eurjchem-2064	255	11	bond	bond	NOUN
eurjchem-2064	255	12	with	with	ADP
eurjchem-2064	255	13	c1	c1	NOUN
eurjchem-2064	255	14	-	-	PUNCT
eurjchem-2064	255	15	s1	s1	NOUN
eurjchem-2064	255	16	-	-	PUNCT
eurjchem-2064	255	17	n1	n1	NOUN
eurjchem-2064	255	18	-	-	PUNCT
eurjchem-2064	255	19	c	c	NOUN
eurjchem-2064	255	20	torsion	torsion	NOUN
eurjchem-2064	255	21	angles	angle	NOUN
eurjchem-2064	255	22	reported	report	VERB
eurjchem-2064	255	23	in	in	ADP
eurjchem-2064	255	24	table	table	NOUN
eurjchem-2064	255	25	4	4	NUM
eurjchem-2064	255	26	.	.	PUNCT
eurjchem-2064	255	27	n	n	CCONJ
eurjchem-2064	255	28	,	,	PUNCT
eurjchem-2064	255	29	n	n	CCONJ
eurjchem-2064	255	30	-	-	PUNCT
eurjchem-2064	255	31	bis(2	bis(2	NOUN
eurjchem-2064	255	32	-	-	PUNCT
eurjchem-2064	255	33	hydroxyethyl)-4	hydroxyethyl)-4	VERB
eurjchem-2064	255	34	-	-	PUNCT
eurjchem-2064	255	35	methylbenzene	methylbenzene	NOUN
eurjchem-2064	255	36	sulfonamide	sulfonamide	NOUN
eurjchem-2064	255	37	(	(	PUNCT
eurjchem-2064	255	38	11	11	NUM
eurjchem-2064	255	39	)	)	PUNCT
eurjchem-2064	255	40	showed	show	VERB
eurjchem-2064	255	41	the	the	DET
eurjchem-2064	255	42	2	2	NUM
eurjchem-2064	255	43	-	-	PUNCT
eurjchem-2064	255	44	hydroxyethyl	hydroxyethyl	NOUN
eurjchem-2064	255	45	and	and	CCONJ
eurjchem-2064	255	46	aryl	aryl	NOUN
eurjchem-2064	255	47	group	group	NOUN
eurjchem-2064	255	48	oriented	orient	VERB
eurjchem-2064	255	49	at	at	ADP
eurjchem-2064	255	50	a	a	DET
eurjchem-2064	255	51	relatively	relatively	ADV
eurjchem-2064	255	52	high	high	ADJ
eurjchem-2064	255	53	c1	c1	NOUN
eurjchem-2064	255	54	-	-	PUNCT
eurjchem-2064	255	55	s1	s1	NOUN
eurjchem-2064	255	56	-	-	PUNCT
eurjchem-2064	255	57	n1	n1	NOUN
eurjchem-2064	255	58	-	-	PUNCT
eurjchem-2064	255	59	c8	c8	NOUN
eurjchem-2064	255	60	torsional	torsional	ADJ
eurjchem-2064	255	61	angle	angle	NOUN
eurjchem-2064	255	62	of	of	ADP
eurjchem-2064	255	63	86.4(2)	86.4(2)	PROPN
eurjchem-2064	255	64	°	°	PROPN
eurjchem-2064	255	65	.	.	PUNCT
eurjchem-2064	256	1	this	this	PRON
eurjchem-2064	256	2	may	may	AUX
eurjchem-2064	256	3	be	be	AUX
eurjchem-2064	256	4	due	due	ADJ
eurjchem-2064	256	5	to	to	ADP
eurjchem-2064	256	6	the	the	DET
eurjchem-2064	256	7	orientation	orientation	NOUN
eurjchem-2064	256	8	of	of	ADP
eurjchem-2064	256	9	the	the	DET
eurjchem-2064	256	10	2hydroxyethyl	2hydroxyethyl	PROPN
eurjchem-2064	256	11	groups	group	NOUN
eurjchem-2064	256	12	,	,	PUNCT
eurjchem-2064	256	13	which	which	PRON
eurjchem-2064	256	14	are	be	AUX
eurjchem-2064	256	15	connected	connect	VERB
eurjchem-2064	256	16	through	through	ADP
eurjchem-2064	256	17	an	an	DET
eurjchem-2064	256	18	intramolecular	intramolecular	ADJ
eurjchem-2064	256	19	hydrogen	hydrogen	NOUN
eurjchem-2064	256	20	bond	bond	NOUN
eurjchem-2064	256	21	.	.	PUNCT
eurjchem-2064	257	1	in	in	ADP
eurjchem-2064	257	2	agreement	agreement	NOUN
eurjchem-2064	257	3	with	with	ADP
eurjchem-2064	257	4	known	know	VERB
eurjchem-2064	257	5	values	value	NOUN
eurjchem-2064	257	6	,	,	PUNCT
eurjchem-2064	257	7	the	the	DET
eurjchem-2064	257	8	s1	s1	NOUN
eurjchem-2064	257	9	=	=	SYM
eurjchem-2064	257	10	o1	o1	NOUN
eurjchem-2064	257	11	and	and	CCONJ
eurjchem-2064	257	12	s1	s1	NOUN
eurjchem-2064	257	13	=	=	SYM
eurjchem-2064	257	14	o2	o2	ADJ
eurjchem-2064	257	15	bond	bond	NOUN
eurjchem-2064	257	16	lengths	length	NOUN
eurjchem-2064	257	17	for	for	ADP
eurjchem-2064	257	18	all	all	DET
eurjchem-2064	257	19	structures	structure	NOUN
eurjchem-2064	257	20	fell	fall	VERB
eurjchem-2064	257	21	within	within	ADP
eurjchem-2064	257	22	the	the	DET
eurjchem-2064	257	23	range	range	NOUN
eurjchem-2064	257	24	of	of	ADP
eurjchem-2064	257	25	1.4251(18)-1.4428(11	1.4251(18)-1.4428(11	NUM
eurjchem-2064	257	26	)	)	PUNCT
eurjchem-2064	257	27	å	å	NOUN
eurjchem-2064	257	28	.	.	PUNCT
eurjchem-2064	258	1	the	the	DET
eurjchem-2064	258	2	c1	c1	PROPN
eurjchem-2064	258	3	-	-	PUNCT
eurjchem-2064	258	4	s1	s1	NOUN
eurjchem-2064	258	5	-	-	PUNCT
eurjchem-2064	258	6	n1	n1	NOUN
eurjchem-2064	258	7	bond	bond	NOUN
eurjchem-2064	258	8	angles	angle	NOUN
eurjchem-2064	258	9	are	be	AUX
eurjchem-2064	258	10	as	as	SCONJ
eurjchem-2064	258	11	follows	follow	VERB
eurjchem-2064	258	12	:	:	PUNCT
eurjchem-2064	258	13	106.84(8	106.84(8	NUM
eurjchem-2064	258	14	)	)	PUNCT
eurjchem-2064	258	15	°	°	PROPN
eurjchem-2064	258	16	,	,	PUNCT
eurjchem-2064	258	17	n	n	CCONJ
eurjchem-2064	258	18	-	-	PUNCT
eurjchem-2064	258	19	benzyl	benzyl	NOUN
eurjchem-2064	258	20	-	-	PUNCT
eurjchem-2064	258	21	n,4	n,4	NUM
eurjchem-2064	258	22	-	-	PUNCT
eurjchem-2064	258	23	dimethyl	dimethyl	NOUN
eurjchem-2064	258	24	benzenesulfonamide	benzenesulfonamide	NOUN
eurjchem-2064	258	25	(	(	PUNCT
eurjchem-2064	258	26	1	1	NUM
eurjchem-2064	258	27	)	)	PUNCT
eurjchem-2064	258	28	;	;	PUNCT
eurjchem-2064	258	29	106.51(9	106.51(9	NUM
eurjchem-2064	258	30	)	)	PUNCT
eurjchem-2064	258	31	°	°	NOUN
eurjchem-2064	258	32	,	,	PUNCT
eurjchem-2064	258	33	4-[(4	4-[(4	NOUN
eurjchem-2064	258	34	-	-	PUNCT
eurjchem-2064	258	35	methylbenzene	methylbenzene	NOUN
eurjchem-2064	258	36	)	)	PUNCT
eurjchem-2064	258	37	sulfonyl]morpholine	sulfonyl]morpholine	PROPN
eurjchem-2064	258	38	(	(	PUNCT
eurjchem-2064	258	39	2	2	NUM
eurjchem-2064	258	40	)	)	PUNCT
eurjchem-2064	258	41	;	;	PUNCT
eurjchem-2064	258	42	107.74(7	107.74(7	NUM
eurjchem-2064	258	43	)	)	PUNCT
eurjchem-2064	258	44	°	°	PROPN
eurjchem-2064	258	45	,	,	PUNCT
eurjchem-2064	258	46	n	n	CCONJ
eurjchem-2064	258	47	-	-	PUNCT
eurjchem-2064	258	48	butyl-4	butyl-4	NOUN
eurjchem-2064	258	49	-	-	PUNCT
eurjchem-2064	258	50	methylbenzene	methylbenzene	NOUN
eurjchem-2064	258	51	sulfonamide	sulfonamide	NOUN
eurjchem-2064	258	52	(	(	PUNCT
eurjchem-2064	258	53	4	4	NUM
eurjchem-2064	258	54	)	)	PUNCT
eurjchem-2064	258	55	;	;	PUNCT
eurjchem-2064	258	56	106.66(7	106.66(7	NUM
eurjchem-2064	258	57	)	)	PUNCT
eurjchem-2064	258	58	°	°	NOUN
eurjchem-2064	258	59	,	,	PUNCT
eurjchem-2064	258	60	1-[(4	1-[(4	NOUN
eurjchem-2064	258	61	-	-	PUNCT
eurjchem-2064	258	62	methyl	methyl	NOUN
eurjchem-2064	258	63	benzene)sulfonyl	benzene)sulfonyl	PROPN
eurjchem-2064	258	64	]	]	X
eurjchem-2064	258	65	piperidine	piperidine	NOUN
eurjchem-2064	258	66	(	(	PUNCT
eurjchem-2064	258	67	5	5	NUM
eurjchem-2064	258	68	)	)	PUNCT
eurjchem-2064	258	69	;	;	PUNCT
eurjchem-2064	258	70	106.57(7	106.57(7	NUM
eurjchem-2064	258	71	)	)	PUNCT
eurjchem-2064	258	72	°	°	PROPN
eurjchem-2064	258	73	,	,	PUNCT
eurjchem-2064	258	74	4	4	NUM
eurjchem-2064	258	75	-	-	PUNCT
eurjchem-2064	258	76	methyl	methyl	NOUN
eurjchem-2064	258	77	-	-	PUNCT
eurjchem-2064	258	78	n	n	CCONJ
eurjchem-2064	258	79	-	-	PUNCT
eurjchem-2064	258	80	phenylbenzenesulfon	phenylbenzenesulfon	NOUN
eurjchem-2064	258	81	amide	amide	NOUN
eurjchem-2064	258	82	(	(	PUNCT
eurjchem-2064	258	83	9	9	NUM
eurjchem-2064	258	84	)	)	PUNCT
eurjchem-2064	258	85	;	;	PUNCT
eurjchem-2064	258	86	106.57(10	106.57(10	X
eurjchem-2064	258	87	)	)	PUNCT
eurjchem-2064	258	88	°	°	PROPN
eurjchem-2064	258	89	,	,	PUNCT
eurjchem-2064	258	90	n	n	CCONJ
eurjchem-2064	258	91	,	,	PUNCT
eurjchem-2064	258	92	n	n	CCONJ
eurjchem-2064	258	93	-	-	PUNCT
eurjchem-2064	258	94	bis(2	bis(2	NOUN
eurjchem-2064	258	95	-	-	PUNCT
eurjchem-2064	258	96	hydroxyethyl)-4	hydroxyethyl)-4	PROPN
eurjchem-2064	258	97	-	-	PUNCT
eurjchem-2064	258	98	methyl	methyl	NOUN
eurjchem-2064	258	99	benzenesulfonamide	benzenesulfonamide	NOUN
eurjchem-2064	258	100	(	(	PUNCT
eurjchem-2064	258	101	11	11	NUM
eurjchem-2064	258	102	)	)	PUNCT
eurjchem-2064	258	103	;	;	PUNCT
eurjchem-2064	258	104	110.29(7	110.29(7	NUM
eurjchem-2064	258	105	)	)	PUNCT
eurjchem-2064	258	106	°	°	NOUN
eurjchem-2064	258	107	,	,	PUNCT
eurjchem-2064	258	108	4	4	NUM
eurjchem-2064	258	109	-	-	PUNCT
eurjchem-2064	258	110	methyl	methyl	NOUN
eurjchem-2064	258	111	-	-	PUNCT
eurjchem-2064	258	112	n-(2,4,4	n-(2,4,4	NOUN
eurjchem-2064	258	113	-	-	ADJ
eurjchem-2064	258	114	tri	tri	ADJ
eurjchem-2064	258	115	methylpentan-2	methylpentan-2	NOUN
eurjchem-2064	258	116	-	-	PUNCT
eurjchem-2064	258	117	yl)benzenesulfonamide	yl)benzenesulfonamide	NOUN
eurjchem-2064	258	118	(	(	PUNCT
eurjchem-2064	258	119	12	12	NUM
eurjchem-2064	258	120	)	)	PUNCT
eurjchem-2064	258	121	.	.	PUNCT
eurjchem-2064	259	1	the	the	DET
eurjchem-2064	259	2	central	central	ADJ
eurjchem-2064	259	3	sulfur	sulfur	NOUN
eurjchem-2064	259	4	atom	atom	NOUN
eurjchem-2064	259	5	,	,	PUNCT
eurjchem-2064	259	6	s1	s1	NOUN
eurjchem-2064	259	7	,	,	PUNCT
eurjchem-2064	259	8	exhibits	exhibit	VERB
eurjchem-2064	259	9	a	a	DET
eurjchem-2064	259	10	slightly	slightly	ADV
eurjchem-2064	259	11	distorted	distort	VERB
eurjchem-2064	259	12	tetrahedron	tetrahedron	NOUN
eurjchem-2064	259	13	geometry	geometry	NOUN
eurjchem-2064	259	14	in	in	ADP
eurjchem-2064	259	15	all	all	DET
eurjchem-2064	259	16	structures	structure	NOUN
eurjchem-2064	259	17	according	accord	VERB
eurjchem-2064	259	18	to	to	ADP
eurjchem-2064	259	19	the	the	DET
eurjchem-2064	259	20	τ4	τ4	NOUN
eurjchem-2064	259	21	descriptor	descriptor	NOUN
eurjchem-2064	259	22	for	for	ADP
eurjchem-2064	259	23	four	four	NUM
eurjchem-2064	259	24	-	-	ADJ
eurjchem-2064	259	25	fold	fold	ADJ
eurjchem-2064	259	26	coordination	coordination	NOUN
eurjchem-2064	259	27	[	[	X
eurjchem-2064	259	28	32	32	NUM
eurjchem-2064	259	29	]	]	PUNCT
eurjchem-2064	259	30	.	.	PUNCT
eurjchem-2064	260	1	two	two	NUM
eurjchem-2064	260	2	of	of	ADP
eurjchem-2064	260	3	the	the	DET
eurjchem-2064	260	4	compounds	compound	NOUN
eurjchem-2064	260	5	,	,	PUNCT
eurjchem-2064	260	6	4-[(4	4-[(4	NOUN
eurjchem-2064	260	7	-	-	PUNCT
eurjchem-2064	260	8	methylbenzene)sulfonyl	methylbenzene)sulfonyl	NOUN
eurjchem-2064	260	9	]	]	X
eurjchem-2064	260	10	morpholine	morpholine	NOUN
eurjchem-2064	260	11	(	(	PUNCT
eurjchem-2064	260	12	2	2	NUM
eurjchem-2064	260	13	)	)	PUNCT
eurjchem-2064	260	14	and	and	CCONJ
eurjchem-2064	260	15	4	4	NUM
eurjchem-2064	260	16	-	-	PUNCT
eurjchem-2064	260	17	methyl	methyl	NOUN
eurjchem-2064	260	18	-	-	PUNCT
eurjchem-2064	260	19	n	n	CCONJ
eurjchem-2064	260	20	-	-	PUNCT
eurjchem-2064	260	21	phenylbenzenesulfonamide	phenylbenzenesulfonamide	NOUN
eurjchem-2064	260	22	(	(	PUNCT
eurjchem-2064	260	23	9	9	NUM
eurjchem-2064	260	24	)	)	PUNCT
eurjchem-2064	260	25	,	,	PUNCT
eurjchem-2064	260	26	have	have	AUX
eurjchem-2064	260	27	previously	previously	ADV
eurjchem-2064	260	28	reported	report	VERB
eurjchem-2064	260	29	crystal	crystal	NOUN
eurjchem-2064	260	30	structures	structure	NOUN
eurjchem-2064	260	31	.	.	PUNCT
eurjchem-2064	261	1	the	the	DET
eurjchem-2064	261	2	packing	packing	NOUN
eurjchem-2064	261	3	polymorph	polymorph	NOUN
eurjchem-2064	261	4	of	of	ADP
eurjchem-2064	261	5	4	4	NUM
eurjchem-2064	261	6	-	-	PUNCT
eurjchem-2064	261	7	methyl	methyl	NOUN
eurjchem-2064	261	8	-	-	PUNCT
eurjchem-2064	261	9	n	n	CCONJ
eurjchem-2064	261	10	-	-	PUNCT
eurjchem-2064	261	11	phenylbenzenesulfonamide	phenylbenzenesulfonamide	NOUN
eurjchem-2064	261	12	has	have	AUX
eurjchem-2064	261	13	been	be	AUX
eurjchem-2064	261	14	reported	report	VERB
eurjchem-2064	261	15	at	at	ADP
eurjchem-2064	261	16	a	a	DET
eurjchem-2064	261	17	temperature	temperature	NOUN
eurjchem-2064	261	18	of	of	ADP
eurjchem-2064	261	19	299	299	NUM
eurjchem-2064	261	20	k	k	NOUN
eurjchem-2064	262	1	[	[	X
eurjchem-2064	262	2	33	33	NUM
eurjchem-2064	262	3	]	]	PUNCT
eurjchem-2064	262	4	.	.	PUNCT
eurjchem-2064	263	1	the	the	DET
eurjchem-2064	263	2	new	new	ADJ
eurjchem-2064	263	3	structure	structure	NOUN
eurjchem-2064	263	4	had	have	VERB
eurjchem-2064	263	5	a	a	DET
eurjchem-2064	263	6	cell	cell	NOUN
eurjchem-2064	263	7	measurement	measurement	NOUN
eurjchem-2064	263	8	temperature	temperature	NOUN
eurjchem-2064	263	9	of	of	ADP
eurjchem-2064	263	10	178	178	NUM
eurjchem-2064	263	11	k.	k.	NOUN
eurjchem-2064	264	1	the	the	DET
eurjchem-2064	264	2	two	two	NUM
eurjchem-2064	264	3	lattices	lattice	NOUN
eurjchem-2064	264	4	'	'	PART
eurjchem-2064	264	5	β	β	X
eurjchem-2064	264	6	unit	unit	NOUN
eurjchem-2064	264	7	cell	cell	NOUN
eurjchem-2064	264	8	angles	angle	NOUN
eurjchem-2064	264	9	differ	differ	VERB
eurjchem-2064	264	10	significantly	significantly	ADV
eurjchem-2064	264	11	.	.	PUNCT
eurjchem-2064	265	1	the	the	DET
eurjchem-2064	265	2	previously	previously	ADV
eurjchem-2064	265	3	reported	report	VERB
eurjchem-2064	265	4	structure	structure	NOUN
eurjchem-2064	265	5	showed	show	VERB
eurjchem-2064	265	6	a	a	DET
eurjchem-2064	265	7	β	β	NOUN
eurjchem-2064	265	8	angle	angle	NOUN
eurjchem-2064	265	9	of	of	ADP
eurjchem-2064	265	10	113.200	113.200	NUM
eurjchem-2064	265	11	(	(	PUNCT
eurjchem-2064	265	12	2	2	NUM
eurjchem-2064	265	13	)	)	PUNCT
eurjchem-2064	265	14	°	°	NOUN
eurjchem-2064	265	15	,	,	PUNCT
eurjchem-2064	265	16	while	while	SCONJ
eurjchem-2064	265	17	the	the	DET
eurjchem-2064	265	18	newly	newly	ADV
eurjchem-2064	265	19	reported	report	VERB
eurjchem-2064	265	20	structure	structure	NOUN
eurjchem-2064	265	21	shows	show	VERB
eurjchem-2064	265	22	β	β	NOUN
eurjchem-2064	265	23	=	=	SYM
eurjchem-2064	265	24	98.8679	98.8679	NUM
eurjchem-2064	265	25	(	(	PUNCT
eurjchem-2064	265	26	7)	7)	NOUN
eurjchem-2064	265	27	°	°	PROPN
eurjchem-2064	265	28	.	.	PUNCT
eurjchem-2064	266	1	additionally	additionally	ADV
eurjchem-2064	266	2	,	,	PUNCT
eurjchem-2064	266	3	the	the	DET
eurjchem-2064	266	4	lengths	length	NOUN
eurjchem-2064	266	5	of	of	ADP
eurjchem-2064	266	6	the	the	DET
eurjchem-2064	266	7	previously	previously	ADV
eurjchem-2064	266	8	reported	report	VERB
eurjchem-2064	266	9	lattice	lattice	PROPN
eurjchem-2064	266	10	unit	unit	NOUN
eurjchem-2064	266	11	cell	cell	NOUN
eurjchem-2064	266	12	were	be	AUX
eurjchem-2064	266	13	a	a	DET
eurjchem-2064	266	14	=	=	NUM
eurjchem-2064	266	15	8.770	8.770	NUM
eurjchem-2064	266	16	(	(	PUNCT
eurjchem-2064	266	17	2	2	NUM
eurjchem-2064	266	18	)	)	PUNCT
eurjchem-2064	266	19	å	å	PROPN
eurjchem-2064	266	20	,	,	PUNCT
eurjchem-2064	266	21	b	b	X
eurjchem-2064	266	22	=	=	SYM
eurjchem-2064	266	23	9.768	9.768	NUM
eurjchem-2064	266	24	(	(	PUNCT
eurjchem-2064	266	25	2	2	NUM
eurjchem-2064	266	26	)	)	PUNCT
eurjchem-2064	266	27	å	å	NOUN
eurjchem-2064	266	28	,	,	PUNCT
eurjchem-2064	266	29	and	and	CCONJ
eurjchem-2064	266	30	c	c	X
eurjchem-2064	266	31	=	=	SYM
eurjchem-2064	266	32	16.234	16.234	NUM
eurjchem-2064	266	33	(	(	PUNCT
eurjchem-2064	266	34	5	5	NUM
eurjchem-2064	266	35	)	)	PUNCT
eurjchem-2064	266	36	å	å	NOUN
eurjchem-2064	266	37	.	.	PUNCT
eurjchem-2064	267	1	the	the	DET
eurjchem-2064	267	2	newly	newly	ADV
eurjchem-2064	267	3	reported	report	VERB
eurjchem-2064	267	4	structure	structure	NOUN
eurjchem-2064	267	5	had	have	VERB
eurjchem-2064	267	6	lengths	length	NOUN
eurjchem-2064	267	7	of	of	ADP
eurjchem-2064	267	8	a	a	DET
eurjchem-2064	267	9	=	=	SYM
eurjchem-2064	267	10	8.6674	8.6674	NUM
eurjchem-2064	267	11	(	(	PUNCT
eurjchem-2064	267	12	1	1	NUM
eurjchem-2064	267	13	)	)	PUNCT
eurjchem-2064	267	14	å	å	PROPN
eurjchem-2064	267	15	,	,	PUNCT
eurjchem-2064	267	16	b	b	NOUN
eurjchem-2064	267	17	=	=	SYM
eurjchem-2064	267	18	9.6925(1	9.6925(1	PROPN
eurjchem-2064	267	19	)	)	PUNCT
eurjchem-2064	267	20	å	å	NOUN
eurjchem-2064	267	21	,	,	PUNCT
eurjchem-2064	267	22	and	and	CCONJ
eurjchem-2064	267	23	c	c	X
eurjchem-2064	267	24	=	=	SYM
eurjchem-2064	267	25	15.1001	15.1001	NUM
eurjchem-2064	267	26	(	(	PUNCT
eurjchem-2064	267	27	2	2	NUM
eurjchem-2064	267	28	)	)	PUNCT
eurjchem-2064	267	29	å	å	NOUN
eurjchem-2064	267	30	.	.	PUNCT
eurjchem-2064	268	1	while	while	SCONJ
eurjchem-2064	268	2	both	both	DET
eurjchem-2064	268	3	structures	structure	NOUN
eurjchem-2064	268	4	are	be	AUX
eurjchem-2064	268	5	oriented	orient	VERB
eurjchem-2064	268	6	gauche	gauche	NOUN
eurjchem-2064	268	7	about	about	ADP
eurjchem-2064	268	8	the	the	DET
eurjchem-2064	268	9	s1	s1	NOUN
eurjchem-2064	268	10	-	-	PUNCT
eurjchem-2064	268	11	n1	n1	NOUN
eurjchem-2064	268	12	bond	bond	NOUN
eurjchem-2064	268	13	,	,	PUNCT
eurjchem-2064	268	14	the	the	DET
eurjchem-2064	268	15	c8	c8	PROPN
eurjchem-2064	268	16	-	-	PUNCT
eurjchem-2064	268	17	n1	n1	NOUN
eurjchem-2064	268	18	-	-	PUNCT
eurjchem-2064	268	19	s1	s1	NOUN
eurjchem-2064	268	20	-	-	PUNCT
eurjchem-2064	268	21	c1	c1	NOUN
eurjchem-2064	268	22	torsional	torsional	ADJ
eurjchem-2064	268	23	angle	angle	NOUN
eurjchem-2064	268	24	differed	differ	VERB
eurjchem-2064	268	25	slightly	slightly	ADV
eurjchem-2064	268	26	.	.	PUNCT
eurjchem-2064	269	1	the	the	DET
eurjchem-2064	269	2	previously	previously	ADV
eurjchem-2064	269	3	reported	report	VERB
eurjchem-2064	269	4	structure	structure	NOUN
eurjchem-2064	269	5	revealed	reveal	VERB
eurjchem-2064	269	6	a	a	DET
eurjchem-2064	269	7	c8	c8	PROPN
eurjchem-2064	269	8	-	-	PUNCT
eurjchem-2064	269	9	n1	n1	NOUN
eurjchem-2064	269	10	-	-	PUNCT
eurjchem-2064	269	11	s1	s1	NOUN
eurjchem-2064	269	12	-	-	PUNCT
eurjchem-2064	269	13	c1	c1	NOUN
eurjchem-2064	269	14	torsional	torsional	ADJ
eurjchem-2064	269	15	angle	angle	NOUN
eurjchem-2064	269	16	of	of	ADP
eurjchem-2064	269	17	-51.6	-51.6	PROPN
eurjchem-2064	269	18	(	(	PUNCT
eurjchem-2064	269	19	3	3	NUM
eurjchem-2064	269	20	)	)	PUNCT
eurjchem-2064	269	21	°	°	NOUN
eurjchem-2064	269	22	,	,	PUNCT
eurjchem-2064	269	23	whereas	whereas	SCONJ
eurjchem-2064	269	24	the	the	DET
eurjchem-2064	269	25	newly	newly	ADV
eurjchem-2064	269	26	obtained	obtain	VERB
eurjchem-2064	269	27	structure	structure	NOUN
eurjchem-2064	269	28	exhibited	exhibit	VERB
eurjchem-2064	269	29	the	the	DET
eurjchem-2064	269	30	same	same	ADJ
eurjchem-2064	269	31	torsional	torsional	ADJ
eurjchem-2064	269	32	angle	angle	NOUN
eurjchem-2064	269	33	as	as	ADP
eurjchem-2064	269	34	-50.6	-50.6	ADJ
eurjchem-2064	269	35	(	(	PUNCT
eurjchem-2064	269	36	1)	1)	NUM
eurjchem-2064	269	37	°	°	NOUN
eurjchem-2064	269	38	.	.	PUNCT
eurjchem-2064	270	1	similarly	similarly	ADV
eurjchem-2064	270	2	,	,	PUNCT
eurjchem-2064	270	3	a	a	DET
eurjchem-2064	270	4	polymorph	polymorph	NOUN
eurjchem-2064	270	5	of	of	ADP
eurjchem-2064	270	6	4-[(4methylbenzene)sulfonyl	4-[(4methylbenzene)sulfonyl	NUM
eurjchem-2064	270	7	]	]	X
eurjchem-2064	270	8	morpholine	morpholine	NOUN
eurjchem-2064	270	9	(	(	PUNCT
eurjchem-2064	270	10	2	2	NUM
eurjchem-2064	270	11	)	)	PUNCT
eurjchem-2064	270	12	has	have	AUX
eurjchem-2064	270	13	been	be	AUX
eurjchem-2064	270	14	previously	previously	ADV
eurjchem-2064	270	15	reported	report	VERB
eurjchem-2064	270	16	at	at	ADP
eurjchem-2064	270	17	a	a	DET
eurjchem-2064	270	18	temperature	temperature	NOUN
eurjchem-2064	270	19	of	of	ADP
eurjchem-2064	270	20	210	210	NUM
eurjchem-2064	270	21	k	k	NOUN
eurjchem-2064	271	1	[	[	X
eurjchem-2064	271	2	34	34	NUM
eurjchem-2064	271	3	]	]	PUNCT
eurjchem-2064	271	4	.	.	PUNCT
eurjchem-2064	272	1	the	the	DET
eurjchem-2064	272	2	new	new	ADJ
eurjchem-2064	272	3	structure	structure	NOUN
eurjchem-2064	272	4	had	have	VERB
eurjchem-2064	272	5	a	a	DET
eurjchem-2064	272	6	cell	cell	NOUN
eurjchem-2064	272	7	measurement	measurement	NOUN
eurjchem-2064	272	8	temperature	temperature	NOUN
eurjchem-2064	272	9	of	of	ADP
eurjchem-2064	272	10	173	173	NUM
eurjchem-2064	272	11	k.	k.	NOUN
eurjchem-2064	272	12	the	the	DET
eurjchem-2064	272	13	previously	previously	ADV
eurjchem-2064	272	14	reported	report	VERB
eurjchem-2064	272	15	structure	structure	NOUN
eurjchem-2064	272	16	had	have	VERB
eurjchem-2064	272	17	unit	unit	NOUN
eurjchem-2064	272	18	cell	cell	NOUN
eurjchem-2064	272	19	lengths	length	NOUN
eurjchem-2064	272	20	of	of	ADP
eurjchem-2064	272	21	a	a	DET
eurjchem-2064	272	22	=	=	SYM
eurjchem-2064	272	23	8.068	8.068	NUM
eurjchem-2064	272	24	(	(	PUNCT
eurjchem-2064	272	25	2	2	NUM
eurjchem-2064	272	26	)	)	PUNCT
eurjchem-2064	272	27	å	å	PROPN
eurjchem-2064	272	28	,	,	PUNCT
eurjchem-2064	272	29	b	b	X
eurjchem-2064	272	30	=	=	SYM
eurjchem-2064	272	31	18.294	18.294	NUM
eurjchem-2064	272	32	(	(	PUNCT
eurjchem-2064	272	33	3	3	NUM
eurjchem-2064	272	34	)	)	PUNCT
eurjchem-2064	272	35	å	å	NOUN
eurjchem-2064	272	36	,	,	PUNCT
eurjchem-2064	272	37	and	and	CCONJ
eurjchem-2064	272	38	c	c	X
eurjchem-2064	272	39	=	=	SYM
eurjchem-2064	272	40	8.815	8.815	NUM
eurjchem-2064	272	41	(	(	PUNCT
eurjchem-2064	272	42	2	2	NUM
eurjchem-2064	272	43	)	)	PUNCT
eurjchem-2064	272	44	å	å	NOUN
eurjchem-2064	272	45	with	with	ADP
eurjchem-2064	272	46	a	a	DET
eurjchem-2064	272	47	β	β	X
eurjchem-2064	272	48	angle	angle	NOUN
eurjchem-2064	272	49	of	of	ADP
eurjchem-2064	272	50	111.694	111.694	NUM
eurjchem-2064	272	51	(	(	PUNCT
eurjchem-2064	272	52	2)	2)	NOUN
eurjchem-2064	272	53	°	°	NOUN
eurjchem-2064	272	54	.	.	PUNCT
eurjchem-2064	273	1	the	the	DET
eurjchem-2064	273	2	new	new	ADJ
eurjchem-2064	273	3	structure	structure	NOUN
eurjchem-2064	273	4	had	have	VERB
eurjchem-2064	273	5	unit	unit	NOUN
eurjchem-2064	273	6	cell	cell	NOUN
eurjchem-2064	273	7	lengths	length	NOUN
eurjchem-2064	273	8	of	of	ADP
eurjchem-2064	273	9	a	a	DET
eurjchem-2064	273	10	=	=	SYM
eurjchem-2064	273	11	8.0852	8.0852	NUM
eurjchem-2064	273	12	(	(	PUNCT
eurjchem-2064	273	13	10	10	NUM
eurjchem-2064	273	14	)	)	PUNCT
eurjchem-2064	273	15	å	å	PROPN
eurjchem-2064	273	16	,	,	PUNCT
eurjchem-2064	273	17	b	b	X
eurjchem-2064	273	18	=	=	SYM
eurjchem-2064	273	19	17.931	17.931	NUM
eurjchem-2064	273	20	(	(	PUNCT
eurjchem-2064	273	21	2	2	NUM
eurjchem-2064	273	22	)	)	PUNCT
eurjchem-2064	273	23	å	å	NOUN
eurjchem-2064	273	24	,	,	PUNCT
eurjchem-2064	273	25	and	and	CCONJ
eurjchem-2064	273	26	c	c	X
eurjchem-2064	273	27	=	=	SYM
eurjchem-2064	273	28	8.7501	8.7501	NUM
eurjchem-2064	273	29	(	(	PUNCT
eurjchem-2064	273	30	11	11	NUM
eurjchem-2064	273	31	)	)	PUNCT
eurjchem-2064	273	32	å	å	NOUN
eurjchem-2064	273	33	with	with	ADP
eurjchem-2064	273	34	a	a	DET
eurjchem-2064	273	35	β	β	NOUN
eurjchem-2064	273	36	angle	angle	NOUN
eurjchem-2064	273	37	of	of	ADP
eurjchem-2064	273	38	111.2125	111.2125	NUM
eurjchem-2064	273	39	(	(	PUNCT
eurjchem-2064	273	40	14)	14)	NUM
eurjchem-2064	273	41	°	°	NOUN
eurjchem-2064	273	42	.	.	PUNCT
eurjchem-2064	274	1	a	a	DET
eurjchem-2064	274	2	notable	notable	ADJ
eurjchem-2064	274	3	difference	difference	NOUN
eurjchem-2064	274	4	in	in	ADP
eurjchem-2064	274	5	the	the	DET
eurjchem-2064	274	6	hydrogen	hydrogen	NOUN
eurjchem-2064	274	7	bond	bond	NOUN
eurjchem-2064	274	8	contact	contact	NOUN
eurjchem-2064	274	9	involving	involve	VERB
eurjchem-2064	274	10	morpholines	morpholine	NOUN
eurjchem-2064	274	11	heteroatoms	heteroatom	NOUN
eurjchem-2064	274	12	was	be	AUX
eurjchem-2064	274	13	noted	note	VERB
eurjchem-2064	274	14	.	.	PUNCT
eurjchem-2064	275	1	the	the	DET
eurjchem-2064	275	2	previous	previous	ADJ
eurjchem-2064	275	3	structure	structure	NOUN
eurjchem-2064	275	4	reported	report	VERB
eurjchem-2064	275	5	a	a	DET
eurjchem-2064	275	6	o3	o3	PROPN
eurjchem-2064	275	7	-	-	PUNCT
eurjchem-2064	275	8	h10a	h10a	PROPN
eurjchem-2064	275	9	hydrogen	hydrogen	NOUN
eurjchem-2064	275	10	bond	bond	NOUN
eurjchem-2064	275	11	contact	contact	NOUN
eurjchem-2064	275	12	length	length	NOUN
eurjchem-2064	275	13	of	of	ADP
eurjchem-2064	275	14	2.794	2.794	NUM
eurjchem-2064	275	15	å	å	NOUN
eurjchem-2064	275	16	,	,	PUNCT
eurjchem-2064	275	17	whereas	whereas	SCONJ
eurjchem-2064	275	18	the	the	DET
eurjchem-2064	275	19	new	new	ADJ
eurjchem-2064	275	20	structure	structure	NOUN
eurjchem-2064	275	21	reported	report	VERB
eurjchem-2064	275	22	a	a	DET
eurjchem-2064	275	23	length	length	NOUN
eurjchem-2064	275	24	of	of	ADP
eurjchem-2064	275	25	2.702	2.702	NUM
eurjchem-2064	275	26	å	å	NOUN
eurjchem-2064	275	27	for	for	ADP
eurjchem-2064	275	28	the	the	DET
eurjchem-2064	275	29	same	same	ADJ
eurjchem-2064	275	30	contact	contact	NOUN
eurjchem-2064	275	31	(	(	PUNCT
eurjchem-2064	275	32	figure	figure	NOUN
eurjchem-2064	275	33	5	5	NUM
eurjchem-2064	275	34	)	)	PUNCT
eurjchem-2064	275	35	.	.	PUNCT
eurjchem-2064	276	1	differences	difference	NOUN
eurjchem-2064	276	2	in	in	ADP
eurjchem-2064	276	3	temperature	temperature	NOUN
eurjchem-2064	276	4	offer	offer	NOUN
eurjchem-2064	276	5	a	a	DET
eurjchem-2064	276	6	suitable	suitable	ADJ
eurjchem-2064	276	7	explanation	explanation	NOUN
eurjchem-2064	276	8	for	for	ADP
eurjchem-2064	276	9	the	the	DET
eurjchem-2064	276	10	conformational	conformational	ADJ
eurjchem-2064	276	11	differences	difference	NOUN
eurjchem-2064	276	12	observed	observe	VERB
eurjchem-2064	276	13	in	in	ADP
eurjchem-2064	276	14	the	the	DET
eurjchem-2064	276	15	polymorphs	polymorphs	NOUN
eurjchem-2064	276	16	.	.	PUNCT
eurjchem-2064	277	1	therefore	therefore	ADV
eurjchem-2064	277	2	,	,	PUNCT
eurjchem-2064	277	3	the	the	DET
eurjchem-2064	277	4	exhibited	exhibit	VERB
eurjchem-2064	277	5	polymorphism	polymorphism	NOUN
eurjchem-2064	277	6	is	be	AUX
eurjchem-2064	277	7	most	most	ADV
eurjchem-2064	277	8	likely	likely	ADJ
eurjchem-2064	277	9	a	a	DET
eurjchem-2064	277	10	result	result	NOUN
eurjchem-2064	277	11	of	of	ADP
eurjchem-2064	277	12	temperature	temperature	NOUN
eurjchem-2064	277	13	dependence	dependence	NOUN
eurjchem-2064	277	14	.	.	PUNCT
eurjchem-2064	278	1	4	4	X
eurjchem-2064	278	2	.	.	X
eurjchem-2064	278	3	conclusion	conclusion	NOUN
eurjchem-2064	278	4	in	in	ADP
eurjchem-2064	278	5	this	this	DET
eurjchem-2064	278	6	work	work	NOUN
eurjchem-2064	278	7	,	,	PUNCT
eurjchem-2064	278	8	methods	method	NOUN
eurjchem-2064	278	9	for	for	ADP
eurjchem-2064	278	10	the	the	DET
eurjchem-2064	278	11	tosylation	tosylation	NOUN
eurjchem-2064	278	12	of	of	ADP
eurjchem-2064	278	13	nitrogen	nitrogen	NOUN
eurjchem-2064	278	14	nucleophiles	nucleophile	NOUN
eurjchem-2064	278	15	using	use	VERB
eurjchem-2064	278	16	various	various	ADJ
eurjchem-2064	278	17	base	base	NOUN
eurjchem-2064	278	18	and	and	CCONJ
eurjchem-2064	278	19	solvent	solvent	ADJ
eurjchem-2064	278	20	combinations	combination	NOUN
eurjchem-2064	278	21	were	be	AUX
eurjchem-2064	278	22	proposed	propose	VERB
eurjchem-2064	278	23	.	.	PUNCT
eurjchem-2064	279	1	the	the	DET
eurjchem-2064	279	2	use	use	NOUN
eurjchem-2064	279	3	of	of	ADP
eurjchem-2064	279	4	aqueous	aqueous	ADJ
eurjchem-2064	279	5	potassium	potassium	NOUN
eurjchem-2064	279	6	carbonate	carbonate	NOUN
eurjchem-2064	279	7	and	and	CCONJ
eurjchem-2064	279	8	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-2064	279	9	gave	give	VERB
eurjchem-2064	279	10	the	the	DET
eurjchem-2064	279	11	best	good	ADJ
eurjchem-2064	279	12	combination	combination	NOUN
eurjchem-2064	279	13	of	of	ADP
eurjchem-2064	279	14	yield	yield	NOUN
eurjchem-2064	279	15	and	and	CCONJ
eurjchem-2064	279	16	reaction	reaction	NOUN
eurjchem-2064	279	17	time	time	NOUN
eurjchem-2064	279	18	.	.	PUNCT
eurjchem-2064	280	1	the	the	DET
eurjchem-2064	280	2	methods	method	NOUN
eurjchem-2064	280	3	were	be	AUX
eurjchem-2064	280	4	useful	useful	ADJ
eurjchem-2064	280	5	in	in	ADP
eurjchem-2064	280	6	producing	produce	VERB
eurjchem-2064	280	7	a	a	DET
eurjchem-2064	280	8	broad	broad	ADJ
eurjchem-2064	280	9	range	range	NOUN
eurjchem-2064	280	10	of	of	ADP
eurjchem-2064	280	11	sulfonamides	sulfonamide	NOUN
eurjchem-2064	280	12	from	from	ADP
eurjchem-2064	280	13	primary	primary	ADJ
eurjchem-2064	280	14	,	,	PUNCT
eurjchem-2064	280	15	secondary	secondary	ADJ
eurjchem-2064	280	16	,	,	PUNCT
eurjchem-2064	280	17	and	and	CCONJ
eurjchem-2064	280	18	heterocyclic	heterocyclic	ADJ
eurjchem-2064	280	19	amines	amine	NOUN
eurjchem-2064	280	20	.	.	PUNCT
eurjchem-2064	281	1	the	the	DET
eurjchem-2064	281	2	ability	ability	NOUN
eurjchem-2064	281	3	to	to	PART
eurjchem-2064	281	4	support	support	VERB
eurjchem-2064	281	5	a	a	DET
eurjchem-2064	281	6	wide	wide	ADJ
eurjchem-2064	281	7	range	range	NOUN
eurjchem-2064	281	8	of	of	ADP
eurjchem-2064	281	9	nitrogen	nitrogen	NOUN
eurjchem-2064	281	10	nucleophiles	nucleophile	NOUN
eurjchem-2064	281	11	allows	allow	VERB
eurjchem-2064	281	12	for	for	ADP
eurjchem-2064	281	13	producing	produce	VERB
eurjchem-2064	281	14	a	a	DET
eurjchem-2064	281	15	variety	variety	NOUN
eurjchem-2064	281	16	of	of	ADP
eurjchem-2064	281	17	biologically	biologically	ADV
eurjchem-2064	281	18	significant	significant	ADJ
eurjchem-2064	281	19	compounds	compound	NOUN
eurjchem-2064	281	20	.	.	PUNCT
eurjchem-2064	282	1	the	the	DET
eurjchem-2064	282	2	new	new	ADJ
eurjchem-2064	282	3	synthetic	synthetic	ADJ
eurjchem-2064	282	4	method	method	NOUN
eurjchem-2064	282	5	resulted	result	VERB
eurjchem-2064	282	6	in	in	ADP
eurjchem-2064	282	7	116	116	NUM
eurjchem-2064	282	8	stenfors	stenfor	NOUN
eurjchem-2064	282	9	and	and	CCONJ
eurjchem-2064	282	10	ngassa	ngassa	NOUN
eurjchem-2064	282	11	/	/	SYM
eurjchem-2064	282	12	european	european	ADJ
eurjchem-2064	282	13	journal	journal	PROPN
eurjchem-2064	282	14	of	of	ADP
eurjchem-2064	282	15	chemistry	chemistry	NOUN
eurjchem-2064	282	16	12	12	NUM
eurjchem-2064	282	17	(	(	PUNCT
eurjchem-2064	282	18	2	2	NUM
eurjchem-2064	282	19	)	)	PUNCT
eurjchem-2064	282	20	(	(	PUNCT
eurjchem-2064	282	21	2021	2021	NUM
eurjchem-2064	282	22	)	)	PUNCT
eurjchem-2064	282	23	109	109	NUM
eurjchem-2064	282	24	-	-	SYM
eurjchem-2064	282	25	116	116	NUM
eurjchem-2064	282	26	2021	2021	NUM
eurjchem-2064	282	27	–	–	PUNCT
eurjchem-2064	282	28	european	european	ADJ
eurjchem-2064	282	29	journal	journal	NOUN
eurjchem-2064	282	30	of	of	ADP
eurjchem-2064	282	31	chemistry	chemistry	NOUN
eurjchem-2064	282	32	–	–	PUNCT
eurjchem-2064	282	33	cc	cc	NOUN
eurjchem-2064	282	34	by	by	ADP
eurjchem-2064	282	35	nc	nc	PROPN
eurjchem-2064	282	36	–	–	PUNCT
eurjchem-2064	282	37	doi	doi	NOUN
eurjchem-2064	282	38	:	:	PUNCT
eurjchem-2064	282	39	10.5155	10.5155	NUM
eurjchem-2064	282	40	/	/	SYM
eurjchem-2064	282	41	eurjchem.12.2.109	eurjchem.12.2.109	NUM
eurjchem-2064	282	42	-	-	PUNCT
eurjchem-2064	282	43	116.2064	116.2064	NUM
eurjchem-2064	282	44	good	good	ADJ
eurjchem-2064	282	45	yields	yield	NOUN
eurjchem-2064	282	46	with	with	ADP
eurjchem-2064	282	47	decreased	decrease	VERB
eurjchem-2064	282	48	environmental	environmental	ADJ
eurjchem-2064	282	49	impact	impact	NOUN
eurjchem-2064	282	50	,	,	PUNCT
eurjchem-2064	282	51	reaction	reaction	NOUN
eurjchem-2064	282	52	time	time	NOUN
eurjchem-2064	282	53	,	,	PUNCT
eurjchem-2064	282	54	and	and	CCONJ
eurjchem-2064	282	55	work	work	NOUN
eurjchem-2064	282	56	-	-	PUNCT
eurjchem-2064	282	57	up	up	NOUN
eurjchem-2064	282	58	over	over	ADP
eurjchem-2064	282	59	the	the	DET
eurjchem-2064	282	60	previous	previous	ADJ
eurjchem-2064	282	61	method	method	NOUN
eurjchem-2064	282	62	.	.	PUNCT
eurjchem-2064	283	1	this	this	DET
eurjchem-2064	283	2	facile	facile	ADJ
eurjchem-2064	283	3	method	method	NOUN
eurjchem-2064	283	4	produced	produce	VERB
eurjchem-2064	283	5	highly	highly	ADV
eurjchem-2064	283	6	pure	pure	ADJ
eurjchem-2064	283	7	sulfonamide	sulfonamide	NOUN
eurjchem-2064	283	8	products	product	NOUN
eurjchem-2064	283	9	and	and	CCONJ
eurjchem-2064	283	10	has	have	VERB
eurjchem-2064	283	11	the	the	DET
eurjchem-2064	283	12	potential	potential	NOUN
eurjchem-2064	283	13	to	to	PART
eurjchem-2064	283	14	create	create	VERB
eurjchem-2064	283	15	a	a	DET
eurjchem-2064	283	16	variety	variety	NOUN
eurjchem-2064	283	17	of	of	ADP
eurjchem-2064	283	18	biologically	biologically	ADV
eurjchem-2064	283	19	significant	significant	ADJ
eurjchem-2064	283	20	compounds	compound	NOUN
eurjchem-2064	283	21	for	for	ADP
eurjchem-2064	283	22	therapeutic	therapeutic	ADJ
eurjchem-2064	283	23	use	use	NOUN
eurjchem-2064	283	24	.	.	PUNCT
eurjchem-2064	284	1	furthermore	furthermore	ADV
eurjchem-2064	284	2	,	,	PUNCT
eurjchem-2064	284	3	crystallographic	crystallographic	ADJ
eurjchem-2064	284	4	characterization	characterization	NOUN
eurjchem-2064	284	5	of	of	ADP
eurjchem-2064	284	6	the	the	DET
eurjchem-2064	284	7	resulting	result	VERB
eurjchem-2064	284	8	structures	structure	NOUN
eurjchem-2064	284	9	revealed	reveal	VERB
eurjchem-2064	284	10	data	datum	NOUN
eurjchem-2064	284	11	for	for	ADP
eurjchem-2064	284	12	five	five	NUM
eurjchem-2064	284	13	novel	novel	ADJ
eurjchem-2064	284	14	structures	structure	NOUN
eurjchem-2064	284	15	and	and	CCONJ
eurjchem-2064	284	16	two	two	NUM
eurjchem-2064	284	17	polymorphs	polymorph	NOUN
eurjchem-2064	284	18	of	of	ADP
eurjchem-2064	284	19	previously	previously	ADV
eurjchem-2064	284	20	reported	report	VERB
eurjchem-2064	284	21	structures	structure	NOUN
eurjchem-2064	284	22	.	.	PUNCT
eurjchem-2064	285	1	this	this	DET
eurjchem-2064	285	2	data	datum	NOUN
eurjchem-2064	285	3	will	will	AUX
eurjchem-2064	285	4	be	be	AUX
eurjchem-2064	285	5	useful	useful	ADJ
eurjchem-2064	285	6	in	in	ADP
eurjchem-2064	285	7	determining	determine	VERB
eurjchem-2064	285	8	the	the	DET
eurjchem-2064	285	9	conformational	conformational	ADJ
eurjchem-2064	285	10	preferences	preference	NOUN
eurjchem-2064	285	11	of	of	ADP
eurjchem-2064	285	12	sulfonamide	sulfonamide	NOUN
eurjchem-2064	285	13	derivatives	derivative	NOUN
eurjchem-2064	285	14	and	and	CCONJ
eurjchem-2064	285	15	predicting	predict	VERB
eurjchem-2064	285	16	their	their	PRON
eurjchem-2064	285	17	structure	structure	NOUN
eurjchem-2064	285	18	-	-	PUNCT
eurjchem-2064	285	19	property	property	NOUN
eurjchem-2064	285	20	relationships	relationship	NOUN
eurjchem-2064	285	21	.	.	PUNCT
eurjchem-2064	286	1	acknowledgements	acknowledgement	NOUN
eurjchem-2064	286	2	the	the	DET
eurjchem-2064	286	3	authors	author	NOUN
eurjchem-2064	286	4	thank	thank	VERB
eurjchem-2064	286	5	pfizer	pfizer	PROPN
eurjchem-2064	286	6	,	,	PUNCT
eurjchem-2064	286	7	inc	inc	PROPN
eurjchem-2064	286	8	.	.	PROPN
eurjchem-2064	286	9	for	for	ADP
eurjchem-2064	286	10	the	the	DET
eurjchem-2064	286	11	donation	donation	NOUN
eurjchem-2064	286	12	of	of	ADP
eurjchem-2064	286	13	a	a	DET
eurjchem-2064	286	14	varian	varian	PROPN
eurjchem-2064	286	15	inova	inova	PROPN
eurjchem-2064	286	16	400	400	NUM
eurjchem-2064	286	17	ft	ft	PROPN
eurjchem-2064	286	18	nmr	nmr	NOUN
eurjchem-2064	286	19	spectrometer	spectrometer	NOUN
eurjchem-2064	286	20	.	.	PUNCT
eurjchem-2064	287	1	the	the	DET
eurjchem-2064	287	2	ccd	ccd	NOUN
eurjchem-2064	287	3	-	-	PUNCT
eurjchem-2064	287	4	based	base	VERB
eurjchem-2064	287	5	x	x	NOUN
eurjchem-2064	287	6	-	-	NOUN
eurjchem-2064	287	7	ray	ray	NOUN
eurjchem-2064	287	8	diffractometers	diffractometer	NOUN
eurjchem-2064	287	9	at	at	ADP
eurjchem-2064	287	10	michigan	michigan	PROPN
eurjchem-2064	287	11	state	state	PROPN
eurjchem-2064	287	12	university	university	PROPN
eurjchem-2064	287	13	were	be	AUX
eurjchem-2064	287	14	upgraded	upgrade	VERB
eurjchem-2064	287	15	and/or	and/or	CCONJ
eurjchem-2064	287	16	replaced	replace	VERB
eurjchem-2064	287	17	by	by	ADP
eurjchem-2064	287	18	departmental	departmental	ADJ
eurjchem-2064	287	19	funds	fund	NOUN
eurjchem-2064	287	20	.	.	PUNCT
eurjchem-2064	288	1	the	the	DET
eurjchem-2064	288	2	authors	author	NOUN
eurjchem-2064	288	3	also	also	ADV
eurjchem-2064	288	4	thank	thank	VERB
eurjchem-2064	288	5	dr	dr	PROPN
eurjchem-2064	288	6	.	.	PROPN
eurjchem-2064	288	7	richard	richard	PROPN
eurjchem-2064	288	8	j.	j.	PROPN
eurjchem-2064	288	9	staples	staples	PROPN
eurjchem-2064	288	10	and	and	CCONJ
eurjchem-2064	288	11	dr	dr	PROPN
eurjchem-2064	288	12	.	.	PROPN
eurjchem-2064	288	13	shannon	shannon	PROPN
eurjchem-2064	288	14	m.	m.	PROPN
eurjchem-2064	288	15	biros	biros	PROPN
eurjchem-2064	288	16	for	for	ADP
eurjchem-2064	288	17	help	help	NOUN
eurjchem-2064	288	18	with	with	ADP
eurjchem-2064	288	19	providing	provide	VERB
eurjchem-2064	288	20	access	access	NOUN
eurjchem-2064	288	21	to	to	ADP
eurjchem-2064	288	22	the	the	DET
eurjchem-2064	288	23	x	x	NOUN
eurjchem-2064	288	24	-	-	NOUN
eurjchem-2064	288	25	ray	ray	NOUN
eurjchem-2064	288	26	diffractometer	diffractometer	NOUN
eurjchem-2064	288	27	at	at	ADP
eurjchem-2064	288	28	michigan	michigan	PROPN
eurjchem-2064	288	29	state	state	PROPN
eurjchem-2064	288	30	university	university	PROPN
eurjchem-2064	288	31	.	.	PUNCT
eurjchem-2064	289	1	supporting	support	VERB
eurjchem-2064	289	2	information	information	NOUN
eurjchem-2064	289	3	ccdc-2054873	ccdc-2054873	NOUN
eurjchem-2064	289	4	(	(	PUNCT
eurjchem-2064	289	5	1	1	NUM
eurjchem-2064	289	6	)	)	PUNCT
eurjchem-2064	289	7	,	,	PUNCT
eurjchem-2064	289	8	2054874	2054874	NUM
eurjchem-2064	289	9	(	(	PUNCT
eurjchem-2064	289	10	2	2	NUM
eurjchem-2064	289	11	)	)	PUNCT
eurjchem-2064	289	12	,	,	PUNCT
eurjchem-2064	289	13	2054875	2054875	NUM
eurjchem-2064	289	14	(	(	PUNCT
eurjchem-2064	289	15	4	4	NUM
eurjchem-2064	289	16	)	)	PUNCT
eurjchem-2064	289	17	,	,	PUNCT
eurjchem-2064	289	18	2054876	2054876	NUM
eurjchem-2064	289	19	(	(	PUNCT
eurjchem-2064	289	20	5	5	NUM
eurjchem-2064	289	21	)	)	PUNCT
eurjchem-2064	289	22	,	,	PUNCT
eurjchem-2064	289	23	2054877	2054877	NUM
eurjchem-2064	289	24	(	(	PUNCT
eurjchem-2064	289	25	9	9	NUM
eurjchem-2064	289	26	)	)	PUNCT
eurjchem-2064	289	27	,	,	PUNCT
eurjchem-2064	289	28	2081811	2081811	NUM
eurjchem-2064	289	29	(	(	PUNCT
eurjchem-2064	289	30	11	11	NUM
eurjchem-2064	289	31	)	)	PUNCT
eurjchem-2064	289	32	and	and	CCONJ
eurjchem-2064	289	33	2081812	2081812	NUM
eurjchem-2064	289	34	(	(	PUNCT
eurjchem-2064	289	35	12	12	NUM
eurjchem-2064	289	36	)	)	PUNCT
eurjchem-2064	289	37	contain	contain	VERB
eurjchem-2064	289	38	the	the	DET
eurjchem-2064	289	39	supplementary	supplementary	ADJ
eurjchem-2064	289	40	crystallographic	crystallographic	ADJ
eurjchem-2064	289	41	data	datum	NOUN
eurjchem-2064	289	42	for	for	ADP
eurjchem-2064	289	43	this	this	DET
eurjchem-2064	289	44	paper	paper	NOUN
eurjchem-2064	289	45	.	.	PUNCT
eurjchem-2064	290	1	these	these	DET
eurjchem-2064	290	2	data	datum	NOUN
eurjchem-2064	290	3	can	can	AUX
eurjchem-2064	290	4	be	be	AUX
eurjchem-2064	290	5	obtained	obtain	VERB
eurjchem-2064	290	6	free	free	ADJ
eurjchem-2064	290	7	of	of	ADP
eurjchem-2064	290	8	charge	charge	NOUN
eurjchem-2064	290	9	via	via	ADP
eurjchem-2064	290	10	https://www.ccdc.cam.ac	https://www.ccdc.cam.ac	NOUN
eurjchem-2064	290	11	.	.	PUNCT
eurjchem-2064	291	1	uk	uk	PROPN
eurjchem-2064	291	2	/	/	SYM
eurjchem-2064	291	3	structures/	structures/	PROPN
eurjchem-2064	291	4	,	,	PUNCT
eurjchem-2064	291	5	or	or	CCONJ
eurjchem-2064	291	6	by	by	ADP
eurjchem-2064	291	7	e	e	NOUN
eurjchem-2064	291	8	-	-	ADJ
eurjchem-2064	291	9	mailing	mailing	ADJ
eurjchem-2064	291	10	data_request@ccdc.cam.ac.uk	data_request@ccdc.cam.ac.uk	PROPN
eurjchem-2064	291	11	,	,	PUNCT
eurjchem-2064	291	12	or	or	CCONJ
eurjchem-2064	291	13	by	by	ADP
eurjchem-2064	291	14	contacting	contact	VERB
eurjchem-2064	291	15	the	the	DET
eurjchem-2064	291	16	cambridge	cambridge	PROPN
eurjchem-2064	291	17	crystallographic	crystallographic	PROPN
eurjchem-2064	291	18	data	data	PROPN
eurjchem-2064	291	19	centre	centre	NOUN
eurjchem-2064	291	20	,	,	PUNCT
eurjchem-2064	291	21	12	12	NUM
eurjchem-2064	291	22	union	union	NOUN
eurjchem-2064	291	23	road	road	NOUN
eurjchem-2064	291	24	,	,	PUNCT
eurjchem-2064	291	25	cambridge	cambridge	PROPN
eurjchem-2064	291	26	cb2	cb2	PROPN
eurjchem-2064	291	27	1ez	1ez	PROPN
eurjchem-2064	291	28	,	,	PUNCT
eurjchem-2064	291	29	uk	uk	PROPN
eurjchem-2064	291	30	;	;	PUNCT
eurjchem-2064	291	31	fax	fax	NOUN
eurjchem-2064	291	32	:	:	PUNCT
eurjchem-2064	291	33	+44(0)1223336033	+44(0)1223336033	PROPN
eurjchem-2064	291	34	.	.	PUNCT
eurjchem-2064	291	35	disclosure	disclosure	NOUN
eurjchem-2064	291	36	statement	statement	NOUN
eurjchem-2064	291	37	conflict	conflict	NOUN
eurjchem-2064	291	38	of	of	ADP
eurjchem-2064	291	39	interests	interest	NOUN
eurjchem-2064	291	40	:	:	PUNCT
eurjchem-2064	291	41	the	the	DET
eurjchem-2064	291	42	authors	author	NOUN
eurjchem-2064	291	43	declare	declare	VERB
eurjchem-2064	291	44	that	that	SCONJ
eurjchem-2064	291	45	they	they	PRON
eurjchem-2064	291	46	have	have	VERB
eurjchem-2064	291	47	no	no	DET
eurjchem-2064	291	48	conflict	conflict	NOUN
eurjchem-2064	291	49	of	of	ADP
eurjchem-2064	291	50	interest	interest	NOUN
eurjchem-2064	291	51	.	.	PUNCT
eurjchem-2064	292	1	author	author	NOUN
eurjchem-2064	292	2	contributions	contribution	NOUN
eurjchem-2064	292	3	:	:	PUNCT
eurjchem-2064	292	4	all	all	DET
eurjchem-2064	292	5	authors	author	NOUN
eurjchem-2064	292	6	contributed	contribute	VERB
eurjchem-2064	292	7	equally	equally	ADV
eurjchem-2064	292	8	to	to	ADP
eurjchem-2064	292	9	this	this	DET
eurjchem-2064	292	10	work	work	NOUN
eurjchem-2064	292	11	.	.	PUNCT
eurjchem-2064	293	1	ethical	ethical	ADJ
eurjchem-2064	293	2	approval	approval	NOUN
eurjchem-2064	293	3	:	:	PUNCT
eurjchem-2064	294	1	all	all	DET
eurjchem-2064	294	2	ethical	ethical	ADJ
eurjchem-2064	294	3	guidelines	guideline	NOUN
eurjchem-2064	294	4	have	have	AUX
eurjchem-2064	294	5	been	be	AUX
eurjchem-2064	294	6	adhered	adhere	VERB
eurjchem-2064	294	7	.	.	PUNCT
eurjchem-2064	295	1	sample	sample	NOUN
eurjchem-2064	295	2	availability	availability	NOUN
eurjchem-2064	295	3	:	:	PUNCT
eurjchem-2064	295	4	sample	sample	NOUN
eurjchem-2064	295	5	of	of	ADP
eurjchem-2064	295	6	the	the	DET
eurjchem-2064	295	7	compounds	compound	NOUN
eurjchem-2064	295	8	are	be	AUX
eurjchem-2064	295	9	available	available	ADJ
eurjchem-2064	295	10	from	from	ADP
eurjchem-2064	295	11	the	the	DET
eurjchem-2064	295	12	author	author	NOUN
eurjchem-2064	295	13	.	.	PUNCT
eurjchem-2064	296	1	funding	funding	NOUN
eurjchem-2064	296	2	funding	funding	NOUN
eurjchem-2064	296	3	for	for	ADP
eurjchem-2064	296	4	this	this	DET
eurjchem-2064	296	5	research	research	NOUN
eurjchem-2064	296	6	was	be	AUX
eurjchem-2064	296	7	provided	provide	VERB
eurjchem-2064	296	8	by	by	ADP
eurjchem-2064	296	9	the	the	DET
eurjchem-2064	296	10	following	following	NOUN
eurjchem-2064	296	11	:	:	PUNCT
eurjchem-2064	296	12	national	national	PROPN
eurjchem-2064	296	13	science	science	PROPN
eurjchem-2064	296	14	foundation	foundation	PROPN
eurjchem-2064	296	15	(	(	PUNCT
eurjchem-2064	296	16	grant	grant	VERB
eurjchem-2064	296	17	no	no	INTJ
eurjchem-2064	296	18	.	.	PUNCT
eurjchem-2064	296	19	mri	mri	NOUN
eurjchem-2064	296	20	che-1725699	che-1725699	NOUN
eurjchem-2064	296	21	)	)	PUNCT
eurjchem-2064	296	22	;	;	PUNCT
eurjchem-2064	296	23	grand	grand	ADJ
eurjchem-2064	296	24	valley	valley	PROPN
eurjchem-2064	296	25	state	state	PROPN
eurjchem-2064	296	26	university	university	PROPN
eurjchem-2064	296	27	chemistry	chemistry	PROPN
eurjchem-2064	296	28	department	department	PROPN
eurjchem-2064	296	29	’s	’s	PART
eurjchem-2064	296	30	weldon	weldon	PROPN
eurjchem-2064	296	31	fund	fund	PROPN
eurjchem-2064	296	32	.	.	PUNCT
eurjchem-2064	297	1	national	national	PROPN
eurjchem-2064	297	2	science	science	PROPN
eurjchem-2064	297	3	foundation	foundation	PROPN
eurjchem-2064	297	4	http://dx.doi.org/10.13039/501100008982	http://dx.doi.org/10.13039/501100008982	PROPN
eurjchem-2064	297	5	orcid	orcid	PROPN
eurjchem-2064	297	6	brock	brock	PROPN
eurjchem-2064	297	7	anton	anton	PROPN
eurjchem-2064	297	8	stenfors	stenfor	NOUN
eurjchem-2064	297	9	https://orcid.org/0000-0001-8760-5878	https://orcid.org/0000-0001-8760-5878	PROPN
eurjchem-2064	297	10	felix	felix	PROPN
eurjchem-2064	297	11	nyuangem	nyuangem	PROPN
eurjchem-2064	297	12	ngassa	ngassa	PROPN
eurjchem-2064	297	13	https://orcid.org/0000-0001-8246-3639	https://orcid.org/0000-0001-8246-3639	PROPN
eurjchem-2064	297	14	references	reference	NOUN
eurjchem-2064	297	15	[	[	X
eurjchem-2064	297	16	1	1	NUM
eurjchem-2064	297	17	]	]	PUNCT
eurjchem-2064	297	18	.	.	PUNCT
eurjchem-2064	298	1	gelmo	gelmo	NOUN
eurjchem-2064	298	2	,	,	PUNCT
eurjchem-2064	298	3	p.	p.	PROPN
eurjchem-2064	298	4	j.	j.	PROPN
eurjchem-2064	298	5	prakt	prakt	PROPN
eurjchem-2064	298	6	.	.	PUNCT
eurjchem-2064	299	1	chem	chem	PROPN
eurjchem-2064	299	2	.	.	PUNCT
eurjchem-2064	300	1	1908	1908	NUM
eurjchem-2064	300	2	,	,	PUNCT
eurjchem-2064	300	3	77	77	NUM
eurjchem-2064	300	4	,	,	PUNCT
eurjchem-2064	300	5	369–382	369–382	NUM
eurjchem-2064	300	6	.	.	PUNCT
eurjchem-2064	301	1	[	[	X
eurjchem-2064	301	2	2	2	NUM
eurjchem-2064	301	3	]	]	PUNCT
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eurjchem-2064	305	7	,	,	PUNCT
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eurjchem-2064	312	2	,	,	PUNCT
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eurjchem-2064	314	29	;	;	PUNCT
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eurjchem-2064	316	2	,	,	PUNCT
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eurjchem-2064	316	4	,	,	PUNCT
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eurjchem-2064	320	2	,	,	PUNCT
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eurjchem-2064	321	4	.	.	PUNCT
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eurjchem-2064	324	8	.	.	PUNCT
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eurjchem-2064	325	4	.	.	PUNCT
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eurjchem-2064	331	2	,	,	PUNCT
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eurjchem-2064	334	2	,	,	PUNCT
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eurjchem-2064	334	4	,	,	PUNCT
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eurjchem-2064	335	4	.	.	PUNCT
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eurjchem-2064	343	2	.	.	PUNCT
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eurjchem-2064	344	2	,	,	PUNCT
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eurjchem-2064	344	4	,	,	PUNCT
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eurjchem-2064	344	6	.	.	PUNCT
eurjchem-2064	345	1	[	[	X
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eurjchem-2064	345	3	]	]	SYM
eurjchem-2064	345	4	.	.	PUNCT
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eurjchem-2064	345	44	,	,	PUNCT
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eurjchem-2064	345	58	p.	p.	NOUN
eurjchem-2064	345	59	;	;	PUNCT
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eurjchem-2064	346	3	]	]	SYM
eurjchem-2064	346	4	.	.	PUNCT
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eurjchem-2064	347	9	.	.	PUNCT
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eurjchem-2064	351	2	.	.	PUNCT
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eurjchem-2064	352	2	,	,	PUNCT
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eurjchem-2064	352	4	,	,	PUNCT
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eurjchem-2064	352	6	–	–	PUNCT
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eurjchem-2064	353	4	.	.	PUNCT
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eurjchem-2064	355	4	.	.	PUNCT
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eurjchem-2064	357	4	.	.	PUNCT
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eurjchem-2064	361	2	,	,	PUNCT
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eurjchem-2064	363	3	,	,	PUNCT
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eurjchem-2064	363	5	,	,	PUNCT
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eurjchem-2064	364	1	[	[	X
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eurjchem-2064	364	4	.	.	PUNCT
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eurjchem-2064	366	2	.	.	PUNCT
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eurjchem-2064	367	2	,	,	PUNCT
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eurjchem-2064	368	4	.	.	PUNCT
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eurjchem-2064	372	4	.	.	PUNCT
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eurjchem-2064	378	2	,	,	PUNCT
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eurjchem-2064	378	4	,	,	PUNCT
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eurjchem-2064	378	6	.	.	PUNCT
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eurjchem-2064	380	25	,	,	PUNCT
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eurjchem-2064	381	2	,	,	PUNCT
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eurjchem-2064	381	4	,	,	PUNCT
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eurjchem-2064	382	2	25	25	NUM
eurjchem-2064	382	3	]	]	PUNCT
eurjchem-2064	382	4	.	.	PUNCT
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eurjchem-2064	383	13	p.	p.	PROPN
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eurjchem-2064	383	26	,	,	PUNCT
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eurjchem-2064	383	38	.	.	PUNCT
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eurjchem-2064	384	3	,	,	PUNCT
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eurjchem-2064	385	4	.	.	PUNCT
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eurjchem-2064	387	3	,	,	PUNCT
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eurjchem-2064	387	5	,	,	PUNCT
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eurjchem-2064	389	4	;	;	PUNCT
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eurjchem-2064	389	21	.	.	PROPN
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eurjchem-2064	390	2	.	.	PUNCT
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eurjchem-2064	391	2	,	,	PUNCT
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eurjchem-2064	392	3	]	]	PUNCT
eurjchem-2064	392	4	.	.	PUNCT
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eurjchem-2064	393	2	,	,	PUNCT
eurjchem-2064	393	3	b.	b.	PROPN
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eurjchem-2064	393	5	;	;	PUNCT
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eurjchem-2064	393	15	;	;	PUNCT
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eurjchem-2064	394	4	.	.	PUNCT
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eurjchem-2064	395	22	.	.	PUNCT
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eurjchem-2064	397	2	.	.	PUNCT
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eurjchem-2064	398	6	.	.	PUNCT
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eurjchem-2064	399	4	.	.	PUNCT
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eurjchem-2064	400	22	.	.	PUNCT
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eurjchem-2064	402	2	.	.	PUNCT
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eurjchem-2064	403	2	,	,	PUNCT
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eurjchem-2064	403	4	,	,	PUNCT
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eurjchem-2064	404	3	]	]	PUNCT
eurjchem-2064	404	4	.	.	PUNCT
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eurjchem-2064	405	2	,	,	PUNCT
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eurjchem-2064	405	5	;	;	PUNCT
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eurjchem-2064	405	23	,	,	PUNCT
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eurjchem-2064	405	33	.	.	PUNCT
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eurjchem-2064	406	3	.	.	PUNCT
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eurjchem-2064	407	2	.	.	PUNCT
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eurjchem-2064	408	2	,	,	PUNCT
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eurjchem-2064	408	4	,	,	PUNCT
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eurjchem-2064	408	6	–	–	PUNCT
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eurjchem-2064	408	8	.	.	PUNCT
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eurjchem-2064	409	4	.	.	PUNCT
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eurjchem-2064	410	2	,	,	PUNCT
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eurjchem-2064	410	4	;	;	PUNCT
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eurjchem-2064	410	6	,	,	PUNCT
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eurjchem-2064	412	5	;	;	PUNCT
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eurjchem-2064	412	7	,	,	PUNCT
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eurjchem-2064	412	16	,	,	PUNCT
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eurjchem-2064	412	21	h.	h.	PROPN
eurjchem-2064	412	22	acta	acta	PROPN
eurjchem-2064	412	23	crystallogr	crystallogr	PROPN
eurjchem-2064	412	24	.	.	PUNCT
eurjchem-2064	413	1	sect	sect	NOUN
eurjchem-2064	413	2	.	.	PUNCT
eurjchem-2064	414	1	e	e	NOUN
eurjchem-2064	414	2	struct	struct	NOUN
eurjchem-2064	414	3	.	.	PUNCT
eurjchem-2064	415	1	rep	rep	PROPN
eurjchem-2064	415	2	.	.	PROPN
eurjchem-2064	415	3	online	online	PROPN
eurjchem-2064	415	4	2009	2009	NUM
eurjchem-2064	415	5	,	,	PUNCT
eurjchem-2064	415	6	65	65	NUM
eurjchem-2064	415	7	,	,	PUNCT
eurjchem-2064	415	8	o1219	o1219	NOUN
eurjchem-2064	415	9	.	.	PUNCT
eurjchem-2064	416	1	[	[	X
eurjchem-2064	416	2	34	34	NUM
eurjchem-2064	416	3	]	]	PUNCT
eurjchem-2064	416	4	.	.	PUNCT
eurjchem-2064	417	1	modarresi	modarresi	PROPN
eurjchem-2064	417	2	-	-	PUNCT
eurjchem-2064	417	3	alam	alam	PROPN
eurjchem-2064	417	4	,	,	PUNCT
eurjchem-2064	417	5	a.	a.	PROPN
eurjchem-2064	417	6	r.	r.	PROPN
eurjchem-2064	417	7	;	;	PUNCT
eurjchem-2064	417	8	amirazizi	amirazizi	PROPN
eurjchem-2064	417	9	,	,	PUNCT
eurjchem-2064	417	10	h.	h.	PROPN
eurjchem-2064	417	11	a.	a.	PROPN
eurjchem-2064	417	12	;	;	PUNCT
eurjchem-2064	417	13	bagheri	bagheri	PROPN
eurjchem-2064	417	14	,	,	PUNCT
eurjchem-2064	417	15	h.	h.	PROPN
eurjchem-2064	417	16	;	;	PUNCT
eurjchem-2064	417	17	bijanzadeh	bijanzadeh	PROPN
eurjchem-2064	417	18	,	,	PUNCT
eurjchem-2064	417	19	h.-r	h.-r	PROPN
eurjchem-2064	417	20	.	.	PUNCT
eurjchem-2064	417	21	;	;	PUNCT
eurjchem-2064	418	1	kleinpeter	kleinpeter	PROPN
eurjchem-2064	418	2	,	,	PUNCT
eurjchem-2064	418	3	e.	e.	PROPN
eurjchem-2064	418	4	j.	j.	PROPN
eurjchem-2064	418	5	org	org	PROPN
eurjchem-2064	418	6	.	.	PUNCT
eurjchem-2064	418	7	chem	chem	PROPN
eurjchem-2064	418	8	.	.	PUNCT
eurjchem-2064	419	1	2009	2009	NUM
eurjchem-2064	419	2	,	,	PUNCT
eurjchem-2064	419	3	74	74	NUM
eurjchem-2064	419	4	,	,	PUNCT
eurjchem-2064	419	5	4740–4746	4740–4746	NUM
eurjchem-2064	419	6	.	.	PUNCT
eurjchem-2064	420	1	copyright	copyright	NOUN
eurjchem-2064	420	2	©	©	PROPN
eurjchem-2064	420	3	2021	2021	NUM
eurjchem-2064	420	4	by	by	ADP
eurjchem-2064	420	5	authors	author	NOUN
eurjchem-2064	420	6	.	.	PUNCT
eurjchem-2064	421	1	this	this	DET
eurjchem-2064	421	2	work	work	NOUN
eurjchem-2064	421	3	is	be	AUX
eurjchem-2064	421	4	published	publish	VERB
eurjchem-2064	421	5	and	and	CCONJ
eurjchem-2064	421	6	licensed	license	VERB
eurjchem-2064	421	7	by	by	ADP
eurjchem-2064	421	8	atlanta	atlanta	PROPN
eurjchem-2064	421	9	publishing	publishing	PROPN
eurjchem-2064	421	10	house	house	PROPN
eurjchem-2064	421	11	llc	llc	PROPN
eurjchem-2064	421	12	,	,	PUNCT
eurjchem-2064	421	13	atlanta	atlanta	PROPN
eurjchem-2064	421	14	,	,	PUNCT
eurjchem-2064	421	15	ga	ga	PROPN
eurjchem-2064	421	16	,	,	PUNCT
eurjchem-2064	421	17	usa	usa	PROPN
eurjchem-2064	421	18	.	.	PUNCT
eurjchem-2064	422	1	the	the	DET
eurjchem-2064	422	2	full	full	ADJ
eurjchem-2064	422	3	terms	term	NOUN
eurjchem-2064	422	4	of	of	ADP
eurjchem-2064	422	5	this	this	DET
eurjchem-2064	422	6	license	license	NOUN
eurjchem-2064	422	7	are	be	AUX
eurjchem-2064	422	8	available	available	ADJ
eurjchem-2064	422	9	at	at	ADP
eurjchem-2064	422	10	http://www.eurjchem.com/index.php/eurjchem/pages/view/terms	http://www.eurjchem.com/index.php/eurjchem/pages/view/term	NOUN
eurjchem-2064	422	11	and	and	CCONJ
eurjchem-2064	422	12	incorporate	incorporate	VERB
eurjchem-2064	422	13	the	the	DET
eurjchem-2064	422	14	creative	creative	ADJ
eurjchem-2064	422	15	commons	common	NOUN
eurjchem-2064	422	16	attribution	attribution	NOUN
eurjchem-2064	422	17	-	-	PUNCT
eurjchem-2064	422	18	non	non	ADJ
eurjchem-2064	422	19	commercial	commercial	NOUN
eurjchem-2064	422	20	(	(	PUNCT
eurjchem-2064	422	21	cc	cc	NOUN
eurjchem-2064	422	22	by	by	ADP
eurjchem-2064	422	23	nc	nc	PROPN
eurjchem-2064	422	24	)	)	PUNCT
eurjchem-2064	422	25	(	(	PUNCT
eurjchem-2064	422	26	international	international	ADJ
eurjchem-2064	422	27	,	,	PUNCT
eurjchem-2064	422	28	v4.0	v4.0	NOUN
eurjchem-2064	422	29	)	)	PUNCT
eurjchem-2064	422	30	license	license	NOUN
eurjchem-2064	422	31	(	(	PUNCT
eurjchem-2064	422	32	http://creativecommons.org/licenses/by-nc/4.0	http://creativecommons.org/licenses/by-nc/4.0	NOUN
eurjchem-2064	422	33	)	)	PUNCT
eurjchem-2064	422	34	.	.	PUNCT
eurjchem-2064	423	1	by	by	ADP
eurjchem-2064	423	2	accessing	access	VERB
eurjchem-2064	423	3	the	the	DET
eurjchem-2064	423	4	work	work	NOUN
eurjchem-2064	423	5	,	,	PUNCT
eurjchem-2064	423	6	you	you	PRON
eurjchem-2064	423	7	hereby	hereby	ADV
eurjchem-2064	423	8	accept	accept	VERB
eurjchem-2064	423	9	the	the	DET
eurjchem-2064	423	10	terms	term	NOUN
eurjchem-2064	423	11	.	.	PUNCT
eurjchem-2064	424	1	this	this	PRON
eurjchem-2064	424	2	is	be	AUX
eurjchem-2064	424	3	an	an	DET
eurjchem-2064	424	4	open	open	ADJ
eurjchem-2064	424	5	access	access	NOUN
eurjchem-2064	424	6	article	article	NOUN
eurjchem-2064	424	7	distributed	distribute	VERB
eurjchem-2064	424	8	under	under	ADP
eurjchem-2064	424	9	the	the	DET
eurjchem-2064	424	10	terms	term	NOUN
eurjchem-2064	424	11	and	and	CCONJ
eurjchem-2064	424	12	conditions	condition	NOUN
eurjchem-2064	424	13	of	of	ADP
eurjchem-2064	424	14	the	the	DET
eurjchem-2064	424	15	cc	cc	PROPN
eurjchem-2064	424	16	by	by	ADP
eurjchem-2064	424	17	nc	nc	PROPN
eurjchem-2064	424	18	license	license	PROPN
eurjchem-2064	424	19	,	,	PUNCT
eurjchem-2064	424	20	which	which	PRON
eurjchem-2064	424	21	permits	permit	VERB
eurjchem-2064	424	22	unrestricted	unrestricted	ADJ
eurjchem-2064	424	23	non	non	ADJ
eurjchem-2064	424	24	-	-	ADJ
eurjchem-2064	424	25	commercial	commercial	ADJ
eurjchem-2064	424	26	use	use	NOUN
eurjchem-2064	424	27	,	,	PUNCT
eurjchem-2064	424	28	distribution	distribution	NOUN
eurjchem-2064	424	29	,	,	PUNCT
eurjchem-2064	424	30	and	and	CCONJ
eurjchem-2064	424	31	reproduction	reproduction	NOUN
eurjchem-2064	424	32	in	in	ADP
eurjchem-2064	424	33	any	any	DET
eurjchem-2064	424	34	medium	medium	NOUN
eurjchem-2064	424	35	,	,	PUNCT
eurjchem-2064	424	36	provided	provide	VERB
eurjchem-2064	424	37	the	the	DET
eurjchem-2064	424	38	original	original	ADJ
eurjchem-2064	424	39	work	work	NOUN
eurjchem-2064	424	40	is	be	AUX
eurjchem-2064	424	41	properly	properly	ADV
eurjchem-2064	424	42	cited	cite	VERB
eurjchem-2064	424	43	without	without	ADP
eurjchem-2064	424	44	any	any	DET
eurjchem-2064	424	45	further	further	ADJ
eurjchem-2064	424	46	permission	permission	NOUN
eurjchem-2064	424	47	from	from	ADP
eurjchem-2064	424	48	atlanta	atlanta	PROPN
eurjchem-2064	424	49	publishing	publishing	PROPN
eurjchem-2064	424	50	house	house	PROPN
eurjchem-2064	424	51	llc	llc	PROPN
eurjchem-2064	424	52	(	(	PUNCT
eurjchem-2064	424	53	european	european	PROPN
eurjchem-2064	424	54	journal	journal	PROPN
eurjchem-2064	424	55	of	of	ADP
eurjchem-2064	424	56	chemistry	chemistry	NOUN
eurjchem-2064	424	57	)	)	PUNCT
eurjchem-2064	424	58	.	.	PUNCT
eurjchem-2064	425	1	no	no	DET
eurjchem-2064	425	2	use	use	NOUN
eurjchem-2064	425	3	,	,	PUNCT
eurjchem-2064	425	4	distribution	distribution	NOUN
eurjchem-2064	425	5	or	or	CCONJ
eurjchem-2064	425	6	reproduction	reproduction	NOUN
eurjchem-2064	425	7	is	be	AUX
eurjchem-2064	425	8	permitted	permit	VERB
eurjchem-2064	425	9	which	which	PRON
eurjchem-2064	425	10	does	do	AUX
eurjchem-2064	425	11	not	not	PART
eurjchem-2064	425	12	comply	comply	VERB
eurjchem-2064	425	13	with	with	ADP
eurjchem-2064	425	14	these	these	DET
eurjchem-2064	425	15	terms	term	NOUN
eurjchem-2064	425	16	.	.	PUNCT
eurjchem-2064	426	1	permissions	permission	NOUN
eurjchem-2064	426	2	for	for	ADP
eurjchem-2064	426	3	commercial	commercial	ADJ
eurjchem-2064	426	4	use	use	NOUN
eurjchem-2064	426	5	of	of	ADP
eurjchem-2064	426	6	this	this	DET
eurjchem-2064	426	7	work	work	NOUN
eurjchem-2064	426	8	beyond	beyond	ADP
eurjchem-2064	426	9	the	the	DET
eurjchem-2064	426	10	scope	scope	NOUN
eurjchem-2064	426	11	of	of	ADP
eurjchem-2064	426	12	the	the	DET
eurjchem-2064	426	13	license	license	NOUN
eurjchem-2064	426	14	(	(	PUNCT
eurjchem-2064	426	15	http://www.eurjchem.com/index.php/eurjchem/pages/view/terms	http://www.eurjchem.com/index.php/eurjchem/pages/view/term	NOUN
eurjchem-2064	426	16	)	)	PUNCT
eurjchem-2064	426	17	are	be	AUX
eurjchem-2064	426	18	administered	administer	VERB
eurjchem-2064	426	19	by	by	ADP
eurjchem-2064	426	20	atlanta	atlanta	PROPN
eurjchem-2064	426	21	publishing	publishing	PROPN
eurjchem-2064	426	22	house	house	PROPN
eurjchem-2064	426	23	llc	llc	PROPN
eurjchem-2064	426	24	(	(	PUNCT
eurjchem-2064	426	25	european	european	PROPN
eurjchem-2064	426	26	journal	journal	PROPN
eurjchem-2064	426	27	of	of	ADP
eurjchem-2064	426	28	chemistry	chemistry	NOUN
eurjchem-2064	426	29	)	)	PUNCT
eurjchem-2064	426	30	.	.	PUNCT
eurjchem-2064	427	1	mailto:data_request@ccdc.cam.ac.uk	mailto:data_request@ccdc.cam.ac.uk	VERB
eurjchem-2064	427	2	http://dx.doi.org/10.13039/501100008982	http://dx.doi.org/10.13039/501100008982	NOUN
eurjchem-2064	427	3	https://orcid.org/0000-0001-8760-5878	https://orcid.org/0000-0001-8760-5878	ADJ
eurjchem-2064	427	4	https://orcid.org/0000-0001-8246-3639	https://orcid.org/0000-0001-8246-3639	NOUN
eurjchem-2064	427	5	http://www.mestrelab.com/	http://www.mestrelab.com/	NOUN
eurjchem-2064	427	6	http://www.eurjchem.com/index.php/eurjchem/pages/view/terms	http://www.eurjchem.com/index.php/eurjchem/pages/view/terms	ADP
eurjchem-2064	427	7	http://creativecommons.org/licenses/by-nc/4.0	http://creativecommons.org/licenses/by-nc/4.0	PROPN
eurjchem-2064	427	8	http://www.eurjchem.com/index.php/eurjchem/pages/view/terms	http://www.eurjchem.com/index.php/eurjchem/pages/view/term	NOUN
eurjchem-2064	427	9	1	1	NUM
eurjchem-2064	427	10	.	.	PUNCT
eurjchem-2064	427	11	introduction	introduction	NOUN
eurjchem-2064	427	12	2	2	NUM
eurjchem-2064	427	13	.	.	PUNCT
eurjchem-2064	427	14	experimental	experimental	ADJ
eurjchem-2064	427	15	2.1	2.1	NUM
eurjchem-2064	427	16	.	.	PUNCT
eurjchem-2064	428	1	synthesis	synthesis	NOUN
eurjchem-2064	428	2	2.1.1	2.1.1	NUM
eurjchem-2064	428	3	.	.	PUNCT
eurjchem-2064	428	4	general	general	ADJ
eurjchem-2064	428	5	procedure	procedure	NOUN
eurjchem-2064	428	6	for	for	ADP
eurjchem-2064	428	7	the	the	DET
eurjchem-2064	428	8	preparation	preparation	NOUN
eurjchem-2064	428	9	of	of	ADP
eurjchem-2064	428	10	sulfonamides	sulfonamide	NOUN
eurjchem-2064	428	11	synthesized	synthesize	VERB
eurjchem-2064	428	12	in	in	ADP
eurjchem-2064	428	13	the	the	DET
eurjchem-2064	428	14	presence	presence	NOUN
eurjchem-2064	428	15	of	of	ADP
eurjchem-2064	428	16	pyridine	pyridine	NOUN
eurjchem-2064	428	17	(	(	PUNCT
eurjchem-2064	428	18	1	1	NUM
eurjchem-2064	428	19	-	-	SYM
eurjchem-2064	428	20	10	10	NUM
eurjchem-2064	428	21	)	)	PUNCT
eurjchem-2064	428	22	2.1.2	2.1.2	NUM
eurjchem-2064	428	23	.	.	PUNCT
eurjchem-2064	428	24	general	general	ADJ
eurjchem-2064	428	25	procedure	procedure	NOUN
eurjchem-2064	428	26	for	for	ADP
eurjchem-2064	428	27	the	the	DET
eurjchem-2064	428	28	preparation	preparation	NOUN
eurjchem-2064	428	29	of	of	ADP
eurjchem-2064	428	30	sulfonamides	sulfonamide	NOUN
eurjchem-2064	428	31	synthesized	synthesize	VERB
eurjchem-2064	428	32	in	in	ADP
eurjchem-2064	428	33	the	the	DET
eurjchem-2064	428	34	presence	presence	NOUN
eurjchem-2064	428	35	of	of	ADP
eurjchem-2064	428	36	potassium	potassium	NOUN
eurjchem-2064	428	37	carbonate	carbonate	NOUN
eurjchem-2064	428	38	(	(	PUNCT
eurjchem-2064	428	39	1	1	NUM
eurjchem-2064	428	40	-	-	SYM
eurjchem-2064	428	41	13	13	NUM
eurjchem-2064	428	42	)	)	PUNCT
eurjchem-2064	428	43	2.1.3	2.1.3	NUM
eurjchem-2064	428	44	.	.	PUNCT
eurjchem-2064	428	45	general	general	ADJ
eurjchem-2064	428	46	procedure	procedure	NOUN
eurjchem-2064	428	47	for	for	ADP
eurjchem-2064	428	48	the	the	DET
eurjchem-2064	428	49	preparation	preparation	NOUN
eurjchem-2064	428	50	of	of	ADP
eurjchem-2064	428	51	sulfonamides	sulfonamide	NOUN
eurjchem-2064	428	52	synthesized	synthesize	VERB
eurjchem-2064	428	53	in	in	ADP
eurjchem-2064	428	54	the	the	DET
eurjchem-2064	428	55	presence	presence	NOUN
eurjchem-2064	428	56	of	of	ADP
eurjchem-2064	428	57	sodium	sodium	NOUN
eurjchem-2064	428	58	hydroxide	hydroxide	NOUN
eurjchem-2064	428	59	(	(	PUNCT
eurjchem-2064	428	60	2	2	NUM
eurjchem-2064	428	61	-	-	SYM
eurjchem-2064	428	62	4	4	NUM
eurjchem-2064	428	63	,	,	PUNCT
eurjchem-2064	428	64	8	8	NUM
eurjchem-2064	428	65	-	-	SYM
eurjchem-2064	428	66	10	10	NUM
eurjchem-2064	428	67	)	)	PUNCT
eurjchem-2064	428	68	2.2	2.2	NUM
eurjchem-2064	428	69	.	.	PUNCT
eurjchem-2064	428	70	crystallographic	crystallographic	ADJ
eurjchem-2064	428	71	characterization	characterization	NOUN
eurjchem-2064	428	72	2.3	2.3	NUM
eurjchem-2064	428	73	.	.	PUNCT
eurjchem-2064	429	1	instrumentation	instrumentation	NOUN
eurjchem-2064	429	2	3	3	NUM
eurjchem-2064	429	3	.	.	NOUN
eurjchem-2064	429	4	results	result	NOUN
eurjchem-2064	429	5	and	and	CCONJ
eurjchem-2064	429	6	discussion	discussion	NOUN
eurjchem-2064	429	7	3.1	3.1	NUM
eurjchem-2064	429	8	.	.	PUNCT
eurjchem-2064	429	9	tosylation	tosylation	NOUN
eurjchem-2064	429	10	of	of	ADP
eurjchem-2064	429	11	amines	amine	NOUN
eurjchem-2064	429	12	3.2	3.2	NUM
eurjchem-2064	429	13	.	.	PUNCT
eurjchem-2064	430	1	isolation	isolation	NOUN
eurjchem-2064	430	2	and	and	CCONJ
eurjchem-2064	430	3	recrystallization	recrystallization	NOUN
eurjchem-2064	430	4	3.3	3.3	NUM
eurjchem-2064	430	5	.	.	PUNCT
eurjchem-2064	431	1	crystallographic	crystallographic	ADJ
eurjchem-2064	431	2	characterization	characterization	NOUN
eurjchem-2064	431	3	4	4	NUM
eurjchem-2064	431	4	.	.	PUNCT
eurjchem-2064	432	1	conclusion	conclusion	NOUN
eurjchem-2064	432	2	acknowledgements	acknowledgement	NOUN
eurjchem-2064	432	3	supporting	support	VERB
eurjchem-2064	432	4	information	information	NOUN
eurjchem-2064	432	5	disclosure	disclosure	NOUN
eurjchem-2064	432	6	statement	statement	NOUN
eurjchem-2064	432	7	funding	fund	VERB
eurjchem-2064	432	8	orcid	orcid	PROPN
eurjchem-2064	432	9	references	reference	NOUN
eurjchem-2064	432	10	printfield10	printfield10	NOUN
eurjchem-2064	432	11	:	:	PUNCT
eurjchem-2064	432	12	printfield11	printfield11	NOUN
eurjchem-2064	432	13	:	:	PUNCT
eurjchem-2064	432	14	printfield12	printfield12	PROPN
eurjchem-2064	432	15	:	:	PUNCT
eurjchem-2064	432	16	printfield13	printfield13	VERB
eurjchem-2064	432	17	:	:	PUNCT
eurjchem-2064	432	18	printfield14	printfield14	NOUN
eurjchem-2064	432	19	:	:	PUNCT
eurjchem-2064	432	20	printfield15	printfield15	NOUN
eurjchem-2064	432	21	:	:	PUNCT
eurjchem-2064	432	22	printfield16	printfield16	ADJ
eurjchem-2064	432	23	:	:	PUNCT
eurjchem-2064	432	24	printfield17	printfield17	NOUN
eurjchem-2064	432	25	:	:	PUNCT
eurjchem-2064	432	26	printfield20	printfield20	PROPN
eurjchem-2064	432	27	:	:	PUNCT
eurjchem-2064	433	1	printfield21	printfield21	ADJ
eurjchem-2064	433	2	:	:	PUNCT
eurjchem-2064	433	3	printfield22	printfield22	NOUN
eurjchem-2064	433	4	:	:	PUNCT
eurjchem-2064	433	5	printfield23	printfield23	NOUN
eurjchem-2064	433	6	:	:	PUNCT
eurjchem-2064	433	7	printfield24	printfield24	NOUN
eurjchem-2064	433	8	:	:	PUNCT
eurjchem-2064	433	9	printfield25	printfield25	NOUN
eurjchem-2064	433	10	:	:	PUNCT
eurjchem-2064	433	11	printfield26	printfield26	ADJ
eurjchem-2064	433	12	:	:	PUNCT
eurjchem-2064	433	13	printfield27	printfield27	NOUN
eurjchem-2064	433	14	:	:	PUNCT