id sid tid token lemma pos eurjchem-207 1 1 microsoft microsoft PROPN eurjchem-207 1 2 word word NOUN eurjchem-207 1 3 european_journal_of_chemistry_1_4_2010_289_290_207 european_journal_of_chemistry_1_4_2010_289_290_207 PROPN eurjchem-207 1 4 european european ADJ eurjchem-207 1 5     SPACE eurjchem-207 1 6 journal journal NOUN eurjchem-207 1 7     SPACE eurjchem-207 1 8 of of ADP eurjchem-207 1 9     SPACE eurjchem-207 1 10 chemistry chemistry NOUN eurjchem-207 1 11     SPACE eurjchem-207 1 12 1 1 NUM eurjchem-207 1 13     SPACE eurjchem-207 1 14 ( ( PUNCT eurjchem-207 1 15 4 4 NUM eurjchem-207 1 16 ) ) PUNCT eurjchem-207 1 17     SPACE eurjchem-207 1 18 ( ( PUNCT eurjchem-207 1 19 2010 2010 NUM eurjchem-207 1 20 ) ) PUNCT eurjchem-207 1 21     SPACE eurjchem-207 1 22 289‐290 289‐290 NUM eurjchem-207 1 23         SPACE eurjchem-207 1 24 european european ADJ eurjchem-207 1 25     SPACE eurjchem-207 1 26 journal journal NOUN eurjchem-207 1 27     SPACE eurjchem-207 1 28 of of ADP eurjchem-207 1 29     SPACE eurjchem-207 1 30 chemistry chemistry NOUN eurjchem-207 1 31     SPACE eurjchem-207 1 32 issn issn VERB eurjchem-207 1 33     SPACE eurjchem-207 1 34 2153‐2249 2153‐2249 NUM eurjchem-207 1 35     SPACE eurjchem-207 1 36 ( ( PUNCT eurjchem-207 1 37 print print NOUN eurjchem-207 1 38 ) ) PUNCT eurjchem-207 1 39     SPACE eurjchem-207 1 40 / / SYM eurjchem-207 1 41     SPACE eurjchem-207 1 42 issn issn VERB eurjchem-207 1 43     SPACE eurjchem-207 1 44 2153‐2257 2153‐2257 NUM eurjchem-207 1 45     SPACE eurjchem-207 1 46 ( ( PUNCT eurjchem-207 1 47 online online ADJ eurjchem-207 1 48 ) ) PUNCT eurjchem-207 1 49     SPACE eurjchem-207 1 50   NOUN eurjchem-207 1 51     SPACE eurjchem-207 1 52 2010 2010 NUM eurjchem-207 1 53     SPACE eurjchem-207 1 54 eurjchem eurjchem NOUN eurjchem-207 1 55     SPACE eurjchem-207 1 56 doi:10.5155 doi:10.5155 PROPN eurjchem-207 1 57 / / SYM eurjchem-207 1 58 eurjchem.1.4.289‐290.207 eurjchem.1.4.289‐290.207 NOUN eurjchem-207 1 59                 SPACE eurjchem-207 1 60 european european ADJ eurjchem-207 1 61     SPACE eurjchem-207 1 62 journal journal NOUN eurjchem-207 1 63     SPACE eurjchem-207 1 64 of of ADP eurjchem-207 1 65     SPACE eurjchem-207 1 66 chemistry chemistry NOUN eurjchem-207 1 67     SPACE eurjchem-207 1 68 journal journal NOUN eurjchem-207 1 69     SPACE eurjchem-207 1 70 homepage homepage NOUN eurjchem-207 1 71 : : PUNCT eurjchem-207 1 72     SPACE eurjchem-207 1 73 www.eurjchem.com www.eurjchem.com NOUN eurjchem-207 1 74                     SPACE eurjchem-207 1 75 synthesis synthesis NOUN eurjchem-207 1 76 , , PUNCT eurjchem-207 1 77     SPACE eurjchem-207 1 78 characterization characterization NOUN eurjchem-207 1 79     SPACE eurjchem-207 1 80 and and CCONJ eurjchem-207 1 81     SPACE eurjchem-207 1 82 crystal crystal NOUN eurjchem-207 1 83     SPACE eurjchem-207 1 84 structure structure NOUN eurjchem-207 1 85     SPACE eurjchem-207 1 86 of of ADP eurjchem-207 1 87       SPACE eurjchem-207 1 88 ethyl ethyl PROPN eurjchem-207 1 89     SPACE eurjchem-207 1 90 4‐(3‐chloro 4‐(3‐chloro PRON eurjchem-207 1 91     SPACE eurjchem-207 1 92 benzamido)benzoate benzamido)benzoate ADJ eurjchem-207 1 93     SPACE eurjchem-207 1 94 aamer aamer ADJ eurjchem-207 1 95     SPACE eurjchem-207 1 96 saeeda saeeda NOUN eurjchem-207 1 97 , , PUNCT eurjchem-207 1 98 * * PUNCT eurjchem-207 1 99 , , PUNCT eurjchem-207 1 100     SPACE eurjchem-207 1 101 hummera hummera NOUN eurjchem-207 1 102     SPACE eurjchem-207 1 103 rafiquea rafiquea NOUN eurjchem-207 1 104     SPACE eurjchem-207 1 105 and and CCONJ eurjchem-207 1 106     SPACE eurjchem-207 1 107 ulrich ulrich NOUN eurjchem-207 1 108     SPACE eurjchem-207 1 109 flörkeb flörkeb VERB eurjchem-207 1 110     SPACE eurjchem-207 1 111 a a DET eurjchem-207 1 112     SPACE eurjchem-207 1 113 department department NOUN eurjchem-207 1 114     SPACE eurjchem-207 1 115 of of ADP eurjchem-207 1 116     SPACE eurjchem-207 1 117 chemistry chemistry NOUN eurjchem-207 1 118 , , PUNCT eurjchem-207 1 119     SPACE eurjchem-207 1 120 quaid­i­azam quaid­i­azam VERB eurjchem-207 1 121     SPACE eurjchem-207 1 122 university university NOUN eurjchem-207 1 123 , , PUNCT eurjchem-207 1 124     SPACE eurjchem-207 1 125 islamabad islamabad PROPN eurjchem-207 1 126 , , PUNCT eurjchem-207 1 127     SPACE eurjchem-207 1 128 pk­45320 pk­45320 PROPN eurjchem-207 1 129 , , PUNCT eurjchem-207 1 130     SPACE eurjchem-207 1 131 pakistan pakistan PROPN eurjchem-207 1 132     SPACE eurjchem-207 1 133 b b PROPN eurjchem-207 1 134     SPACE eurjchem-207 1 135 department department NOUN eurjchem-207 1 136     SPACE eurjchem-207 1 137 chemie chemie PROPN eurjchem-207 1 138 , , PUNCT eurjchem-207 1 139     SPACE eurjchem-207 1 140 fakultät fakultät ADJ eurjchem-207 1 141     SPACE eurjchem-207 1 142 fur fur NOUN eurjchem-207 1 143     SPACE eurjchem-207 1 144 naturwissenschaften naturwissenschaften NOUN eurjchem-207 1 145 , , PUNCT eurjchem-207 1 146     SPACE eurjchem-207 1 147 universitat universitat X eurjchem-207 1 148     SPACE eurjchem-207 1 149 paderborn paderborn ADJ eurjchem-207 1 150 , , PUNCT eurjchem-207 1 151     SPACE eurjchem-207 1 152 warburgerstrasse warburgerstrasse NOUN eurjchem-207 1 153     SPACE eurjchem-207 1 154 100 100 NUM eurjchem-207 1 155 , , PUNCT eurjchem-207 1 156     SPACE eurjchem-207 1 157 paderborn paderborn ADJ eurjchem-207 1 158 , , PUNCT eurjchem-207 1 159     SPACE eurjchem-207 1 160 d­33098 d­33098 NOUN eurjchem-207 1 161 , , PUNCT eurjchem-207 1 162     SPACE eurjchem-207 1 163 germany germany PROPN eurjchem-207 1 164     SPACE eurjchem-207 1 165 * * PROPN eurjchem-207 1 166 corresponding corresponding ADJ eurjchem-207 1 167     SPACE eurjchem-207 1 168 author author NOUN eurjchem-207 1 169     SPACE eurjchem-207 1 170 at at ADP eurjchem-207 1 171 : : PUNCT eurjchem-207 1 172     SPACE eurjchem-207 1 173 department department NOUN eurjchem-207 1 174     SPACE eurjchem-207 1 175 of of ADP eurjchem-207 1 176     SPACE eurjchem-207 1 177 chemistry chemistry NOUN eurjchem-207 1 178 , , PUNCT eurjchem-207 1 179     SPACE eurjchem-207 1 180 quaid­i­azam quaid­i­azam VERB eurjchem-207 1 181     SPACE eurjchem-207 1 182 university university NOUN eurjchem-207 1 183 , , PUNCT eurjchem-207 1 184     SPACE eurjchem-207 1 185 islamabad islamabad PROPN eurjchem-207 1 186 , , PUNCT eurjchem-207 1 187     SPACE eurjchem-207 1 188 pk­45320 pk­45320 PROPN eurjchem-207 1 189 , , PUNCT eurjchem-207 1 190     SPACE eurjchem-207 1 191 pakistan pakistan PROPN eurjchem-207 1 192 . . PUNCT eurjchem-207 1 193     SPACE eurjchem-207 2 1 tel tel PROPN eurjchem-207 2 2 . . PUNCT eurjchem-207 2 3 : : PUNCT eurjchem-207 2 4     SPACE eurjchem-207 2 5 +92.51.90642128 +92.51.90642128 ADP eurjchem-207 2 6 ; ; PUNCT eurjchem-207 2 7     SPACE eurjchem-207 2 8 fax fax NOUN eurjchem-207 2 9 : : PUNCT eurjchem-207 2 10     SPACE eurjchem-207 2 11 +92.51.90642241 +92.51.90642241 PROPN eurjchem-207 2 12 . . PUNCT eurjchem-207 2 13     SPACE eurjchem-207 2 14 e­mail e­mail NOUN eurjchem-207 2 15     SPACE eurjchem-207 2 16 address address NOUN eurjchem-207 2 17 : : PUNCT eurjchem-207 2 18     SPACE eurjchem-207 2 19 aamersaeed@yahoo.com aamersaeed@yahoo.com X eurjchem-207 2 20     SPACE eurjchem-207 2 21 ( ( PUNCT eurjchem-207 2 22 a. a. NOUN eurjchem-207 2 23     SPACE eurjchem-207 2 24 saeed saeed PROPN eurjchem-207 2 25 ) ) PUNCT eurjchem-207 2 26 . . PUNCT eurjchem-207 2 27                                 SPACE eurjchem-207 2 28 article article NOUN eurjchem-207 2 29     SPACE eurjchem-207 2 30 information information NOUN eurjchem-207 2 31         SPACE eurjchem-207 2 32 abstract abstract ADJ eurjchem-207 2 33 received receive VERB eurjchem-207 2 34 : : PUNCT eurjchem-207 2 35     SPACE eurjchem-207 2 36 15 15 NUM eurjchem-207 2 37     SPACE eurjchem-207 2 38 july july PROPN eurjchem-207 2 39     SPACE eurjchem-207 2 40 2010 2010 NUM eurjchem-207 2 41     SPACE eurjchem-207 2 42 accepted accept VERB eurjchem-207 2 43 : : PUNCT eurjchem-207 2 44     SPACE eurjchem-207 2 45 07 07 NUM eurjchem-207 2 46     SPACE eurjchem-207 2 47 august august PROPN eurjchem-207 2 48     SPACE eurjchem-207 2 49 2010 2010 NUM eurjchem-207 2 50     SPACE eurjchem-207 2 51 online online NOUN eurjchem-207 2 52 : : PUNCT eurjchem-207 2 53     SPACE eurjchem-207 2 54 31 31 NUM eurjchem-207 2 55     SPACE eurjchem-207 2 56 december december PROPN eurjchem-207 2 57     SPACE eurjchem-207 2 58 2010 2010 NUM eurjchem-207 2 59     SPACE eurjchem-207 2 60 keywords keyword VERB eurjchem-207 2 61         SPACE eurjchem-207 2 62 the the DET eurjchem-207 2 63     SPACE eurjchem-207 2 64 title title NOUN eurjchem-207 2 65     SPACE eurjchem-207 2 66 compound compound NOUN eurjchem-207 2 67     SPACE eurjchem-207 2 68 was be AUX eurjchem-207 2 69     SPACE eurjchem-207 2 70 efficiently efficiently ADV eurjchem-207 2 71     SPACE eurjchem-207 2 72 synthesized synthesize VERB eurjchem-207 2 73     SPACE eurjchem-207 2 74 in in ADP eurjchem-207 2 75     SPACE eurjchem-207 2 76 two two NUM eurjchem-207 2 77     SPACE eurjchem-207 2 78 steps step NOUN eurjchem-207 2 79     SPACE eurjchem-207 2 80 starting start VERB eurjchem-207 2 81     SPACE eurjchem-207 2 82 from from ADP eurjchem-207 2 83     SPACE eurjchem-207 2 84 esterification esterification NOUN eurjchem-207 2 85     SPACE eurjchem-207 2 86 of of ADP eurjchem-207 2 87     SPACE eurjchem-207 2 88 4‐aminobenzoic 4‐aminobenzoic ADJ eurjchem-207 2 89     SPACE eurjchem-207 2 90 acid acid NOUN eurjchem-207 2 91     SPACE eurjchem-207 2 92 followed follow VERB eurjchem-207 2 93     SPACE eurjchem-207 2 94 by by ADP eurjchem-207 2 95     SPACE eurjchem-207 2 96 amidation amidation NOUN eurjchem-207 2 97     SPACE eurjchem-207 2 98 with with ADP eurjchem-207 2 99     SPACE eurjchem-207 2 100 3‐chlorobenzoyl 3‐chlorobenzoyl PROPN eurjchem-207 2 101     SPACE eurjchem-207 2 102 chloride chloride NOUN eurjchem-207 2 103     SPACE eurjchem-207 2 104 in in ADP eurjchem-207 2 105     SPACE eurjchem-207 2 106 dry dry ADJ eurjchem-207 2 107     SPACE eurjchem-207 2 108 tetrahydrofuran tetrahydrofuran NOUN eurjchem-207 2 109 . . PUNCT eurjchem-207 2 110     SPACE eurjchem-207 3 1 the the DET eurjchem-207 3 2     SPACE eurjchem-207 3 3 structure structure NOUN eurjchem-207 3 4     SPACE eurjchem-207 3 5 was be AUX eurjchem-207 3 6     SPACE eurjchem-207 3 7 confirmed confirm VERB eurjchem-207 3 8     SPACE eurjchem-207 3 9 by by ADP eurjchem-207 3 10     SPACE eurjchem-207 3 11 spectroscopic spectroscopic NOUN eurjchem-207 3 12     SPACE eurjchem-207 3 13 data datum NOUN eurjchem-207 3 14     SPACE eurjchem-207 3 15 and and CCONJ eurjchem-207 3 16     SPACE eurjchem-207 3 17 elemental elemental NOUN eurjchem-207 3 18     SPACE eurjchem-207 3 19 analysis analysis NOUN eurjchem-207 3 20 . . PUNCT eurjchem-207 3 21     SPACE eurjchem-207 4 1 the the DET eurjchem-207 4 2     SPACE eurjchem-207 4 3 molecular molecular ADJ eurjchem-207 4 4     SPACE eurjchem-207 4 5 structure structure NOUN eurjchem-207 4 6     SPACE eurjchem-207 4 7 was be AUX eurjchem-207 4 8     SPACE eurjchem-207 4 9 determined determine VERB eurjchem-207 4 10     SPACE eurjchem-207 4 11 from from ADP eurjchem-207 4 12     SPACE eurjchem-207 4 13 single single ADJ eurjchem-207 4 14     SPACE eurjchem-207 4 15 crystal crystal NOUN eurjchem-207 4 16     SPACE eurjchem-207 4 17 x‐ray x‐ray PROPN eurjchem-207 4 18     SPACE eurjchem-207 4 19 diffraction diffraction NOUN eurjchem-207 4 20     SPACE eurjchem-207 4 21 data datum NOUN eurjchem-207 4 22 . . PUNCT eurjchem-207 4 23     SPACE eurjchem-207 5 1 it it PRON eurjchem-207 5 2     SPACE eurjchem-207 5 3 crystallizes crystallize VERB eurjchem-207 5 4     SPACE eurjchem-207 5 5 in in ADP eurjchem-207 5 6     SPACE eurjchem-207 5 7 the the DET eurjchem-207 5 8     SPACE eurjchem-207 5 9 triclinic triclinic ADJ eurjchem-207 5 10     SPACE eurjchem-207 5 11 space space NOUN eurjchem-207 5 12     SPACE eurjchem-207 5 13 group group NOUN eurjchem-207 5 14     SPACE eurjchem-207 5 15 p‐1 p‐1 VERB eurjchem-207 5 16     SPACE eurjchem-207 5 17 with with ADP eurjchem-207 5 18     SPACE eurjchem-207 5 19 z z NOUN eurjchem-207 5 20     SPACE eurjchem-207 5 21 = = NOUN eurjchem-207 5 22     SPACE eurjchem-207 5 23 2 2 NUM eurjchem-207 5 24     SPACE eurjchem-207 5 25 and and CCONJ eurjchem-207 5 26     SPACE eurjchem-207 5 27 unit unit NOUN eurjchem-207 5 28     SPACE eurjchem-207 5 29 cell cell NOUN eurjchem-207 5 30     SPACE eurjchem-207 5 31 dimensions dimension NOUN eurjchem-207 5 32     SPACE eurjchem-207 5 33 a a DET eurjchem-207 5 34     SPACE eurjchem-207 5 35 = = NOUN eurjchem-207 5 36     SPACE eurjchem-207 5 37 5.2941(15 5.2941(15 NUM eurjchem-207 5 38 ) ) PUNCT eurjchem-207 5 39     SPACE eurjchem-207 5 40 å å PROPN eurjchem-207 5 41 , , PUNCT eurjchem-207 5 42     SPACE eurjchem-207 5 43 b b NOUN eurjchem-207 5 44     SPACE eurjchem-207 5 45 = = NOUN eurjchem-207 5 46     SPACE eurjchem-207 5 47 8.157(2 8.157(2 NUM eurjchem-207 5 48 ) ) PUNCT eurjchem-207 5 49     SPACE eurjchem-207 5 50 å å PROPN eurjchem-207 5 51 , , PUNCT eurjchem-207 5 52     SPACE eurjchem-207 5 53 c c NOUN eurjchem-207 5 54     SPACE eurjchem-207 5 55 = = NOUN eurjchem-207 5 56     SPACE eurjchem-207 5 57 16.238(4 16.238(4 NOUN eurjchem-207 5 58 ) ) PUNCT eurjchem-207 5 59     SPACE eurjchem-207 5 60 å å PROPN eurjchem-207 5 61 , , PUNCT eurjchem-207 5 62     SPACE eurjchem-207 5 63 α α NOUN eurjchem-207 5 64     SPACE eurjchem-207 5 65 = = NOUN eurjchem-207 5 66     SPACE eurjchem-207 5 67 82.682(6 82.682(6 NOUN eurjchem-207 5 68 ) ) PUNCT eurjchem-207 5 69 ° ° PROPN eurjchem-207 5 70 , , PUNCT eurjchem-207 5 71     SPACE eurjchem-207 5 72 β β VERB eurjchem-207 5 73     SPACE eurjchem-207 5 74 = = NOUN eurjchem-207 5 75     SPACE eurjchem-207 5 76 84.481(6 84.481(6 NUM eurjchem-207 5 77 ) ) PUNCT eurjchem-207 5 78 ° ° NOUN eurjchem-207 5 79 , , PUNCT eurjchem-207 5 80     SPACE eurjchem-207 5 81 γ γ PROPN eurjchem-207 5 82     SPACE eurjchem-207 5 83 = = NOUN eurjchem-207 5 84     SPACE eurjchem-207 5 85 80.100(6 80.100(6 NOUN eurjchem-207 5 86 ) ) PUNCT eurjchem-207 5 87 ° ° NOUN eurjchem-207 5 88     SPACE eurjchem-207 5 89 and and CCONJ eurjchem-207 5 90     SPACE eurjchem-207 5 91 v v NOUN eurjchem-207 5 92     SPACE eurjchem-207 5 93 = = NOUN eurjchem-207 5 94     SPACE eurjchem-207 5 95 683.2(3 683.2(3 NOUN eurjchem-207 5 96 ) ) PUNCT eurjchem-207 5 97     SPACE eurjchem-207 5 98 å3 å3 PROPN eurjchem-207 5 99 . . PUNCT eurjchem-207 5 100     SPACE eurjchem-207 5 101 ethyl ethyl PROPN eurjchem-207 5 102     SPACE eurjchem-207 5 103 4‐(3‐chlorobenzamido)benzoate 4‐(3‐chlorobenzamido)benzoate PROPN eurjchem-207 5 104     SPACE eurjchem-207 5 105 crystal crystal NOUN eurjchem-207 5 106     SPACE eurjchem-207 5 107 structure structure NOUN eurjchem-207 5 108     SPACE eurjchem-207 5 109 synthesis synthesis NOUN eurjchem-207 5 110     SPACE eurjchem-207 5 111 characterization characterization NOUN eurjchem-207 5 112         SPACE eurjchem-207 5 113 1 1 NUM eurjchem-207 5 114 . . PUNCT eurjchem-207 5 115     SPACE eurjchem-207 5 116 introduction introduction NOUN eurjchem-207 5 117         SPACE eurjchem-207 5 118 ethyl ethyl PROPN eurjchem-207 5 119     SPACE eurjchem-207 5 120 4‐(3‐chlorobenzamido)benzoate 4‐(3‐chlorobenzamido)benzoate NOUN eurjchem-207 5 121     SPACE eurjchem-207 5 122 is be AUX eurjchem-207 5 123     SPACE eurjchem-207 5 124 an an DET eurjchem-207 5 125     SPACE eurjchem-207 5 126 exceptionally exceptionally ADV eurjchem-207 5 127     SPACE eurjchem-207 5 128 important important ADJ eurjchem-207 5 129     SPACE eurjchem-207 5 130 intermediate intermediate ADJ eurjchem-207 5 131     SPACE eurjchem-207 5 132 towards towards ADP eurjchem-207 5 133     SPACE eurjchem-207 5 134 the the DET eurjchem-207 5 135     SPACE eurjchem-207 5 136 synthesis synthesis NOUN eurjchem-207 5 137     SPACE eurjchem-207 5 138 of of ADP eurjchem-207 5 139     SPACE eurjchem-207 5 140 a a DET eurjchem-207 5 141     SPACE eurjchem-207 5 142 variety variety NOUN eurjchem-207 5 143     SPACE eurjchem-207 5 144 of of ADP eurjchem-207 5 145     SPACE eurjchem-207 5 146 heterocyclic heterocyclic NOUN eurjchem-207 5 147     SPACE eurjchem-207 5 148 compounds compound NOUN eurjchem-207 5 149     SPACE eurjchem-207 5 150 including include VERB eurjchem-207 5 151     SPACE eurjchem-207 5 152 1,3,4‐oxadiazoles 1,3,4‐oxadiazole NOUN eurjchem-207 5 153 , , PUNCT eurjchem-207 5 154     SPACE eurjchem-207 5 155 1,2,4‐ 1,2,4‐ NUM eurjchem-207 5 156 triazoles triazole NOUN eurjchem-207 5 157 , , PUNCT eurjchem-207 5 158     SPACE eurjchem-207 5 159 1,3,4‐thiadiazoles 1,3,4‐thiadiazoles PROPN eurjchem-207 5 160     SPACE eurjchem-207 5 161 and and CCONJ eurjchem-207 5 162     SPACE eurjchem-207 5 163 1,2,4‐triazines 1,2,4‐triazine NOUN eurjchem-207 5 164 , , PUNCT eurjchem-207 5 165     SPACE eurjchem-207 5 166 all all PRON eurjchem-207 5 167     SPACE eurjchem-207 5 168 of of ADP eurjchem-207 5 169     SPACE eurjchem-207 5 170 which which PRON eurjchem-207 5 171     SPACE eurjchem-207 5 172 exhibit exhibit VERB eurjchem-207 5 173     SPACE eurjchem-207 5 174 a a DET eurjchem-207 5 175     SPACE eurjchem-207 5 176 wide wide ADJ eurjchem-207 5 177     SPACE eurjchem-207 5 178 spectrum spectrum NOUN eurjchem-207 5 179     SPACE eurjchem-207 5 180 of of ADP eurjchem-207 5 181     SPACE eurjchem-207 5 182 bioactivities bioactivitie NOUN eurjchem-207 5 183     SPACE eurjchem-207 5 184 [ [ X eurjchem-207 5 185 1‐4 1‐4 NOUN eurjchem-207 5 186 ] ] PUNCT eurjchem-207 5 187 . . PUNCT eurjchem-207 5 188     SPACE eurjchem-207 6 1 the the DET eurjchem-207 6 2     SPACE eurjchem-207 6 3 benzanilide benzanilide NOUN eurjchem-207 6 4     SPACE eurjchem-207 6 5 core core NOUN eurjchem-207 6 6     SPACE eurjchem-207 6 7 is be AUX eurjchem-207 6 8     SPACE eurjchem-207 6 9 present present ADJ eurjchem-207 6 10     SPACE eurjchem-207 6 11 in in ADP eurjchem-207 6 12     SPACE eurjchem-207 6 13 compounds compound NOUN eurjchem-207 6 14     SPACE eurjchem-207 6 15 with with ADP eurjchem-207 6 16     SPACE eurjchem-207 6 17 such such ADJ eurjchem-207 6 18     SPACE eurjchem-207 6 19 a a DET eurjchem-207 6 20     SPACE eurjchem-207 6 21 wide wide ADJ eurjchem-207 6 22     SPACE eurjchem-207 6 23 range range NOUN eurjchem-207 6 24     SPACE eurjchem-207 6 25 of of ADP eurjchem-207 6 26     SPACE eurjchem-207 6 27 biological biological ADJ eurjchem-207 6 28     SPACE eurjchem-207 6 29 activities activity NOUN eurjchem-207 6 30     SPACE eurjchem-207 6 31 that that SCONJ eurjchem-207 6 32     SPACE eurjchem-207 6 33 it it PRON eurjchem-207 6 34     SPACE eurjchem-207 6 35 has have AUX eurjchem-207 6 36     SPACE eurjchem-207 6 37 been be AUX eurjchem-207 6 38     SPACE eurjchem-207 6 39 called call VERB eurjchem-207 6 40     SPACE eurjchem-207 6 41 a a DET eurjchem-207 6 42     SPACE eurjchem-207 6 43 privileged privileged ADJ eurjchem-207 6 44     SPACE eurjchem-207 6 45 structure structure NOUN eurjchem-207 6 46 . . PUNCT eurjchem-207 6 47     SPACE eurjchem-207 7 1 benzanilides benzanilide NOUN eurjchem-207 7 2     SPACE eurjchem-207 7 3 have have AUX eurjchem-207 7 4     SPACE eurjchem-207 7 5 established establish VERB eurjchem-207 7 6     SPACE eurjchem-207 7 7 their their PRON eurjchem-207 7 8     SPACE eurjchem-207 7 9 efficacy efficacy NOUN eurjchem-207 7 10     SPACE eurjchem-207 7 11 as as ADP eurjchem-207 7 12     SPACE eurjchem-207 7 13 centroid centroid NOUN eurjchem-207 7 14     SPACE eurjchem-207 7 15 elements element NOUN eurjchem-207 7 16     SPACE eurjchem-207 7 17 of of ADP eurjchem-207 7 18     SPACE eurjchem-207 7 19 ligands ligand NOUN eurjchem-207 7 20     SPACE eurjchem-207 7 21 that that SCONJ eurjchem-207 7 22     SPACE eurjchem-207 7 23 bind bind VERB eurjchem-207 7 24     SPACE eurjchem-207 7 25 to to ADP eurjchem-207 7 26     SPACE eurjchem-207 7 27 a a DET eurjchem-207 7 28     SPACE eurjchem-207 7 29 wide wide ADJ eurjchem-207 7 30     SPACE eurjchem-207 7 31 variety variety NOUN eurjchem-207 7 32     SPACE eurjchem-207 7 33 of of ADP eurjchem-207 7 34     SPACE eurjchem-207 7 35 receptor receptor NOUN eurjchem-207 7 36     SPACE eurjchem-207 7 37 types type NOUN eurjchem-207 7 38     SPACE eurjchem-207 8 1 [ [ X eurjchem-207 8 2 5 5 NUM eurjchem-207 8 3 ] ] PUNCT eurjchem-207 8 4 . . PUNCT eurjchem-207 8 5     SPACE eurjchem-207 8 6 imatinib imatinib NOUN eurjchem-207 8 7     SPACE eurjchem-207 8 8 is be AUX eurjchem-207 8 9     SPACE eurjchem-207 8 10 a a DET eurjchem-207 8 11     SPACE eurjchem-207 8 12 drug drug NOUN eurjchem-207 8 13     SPACE eurjchem-207 8 14 used use VERB eurjchem-207 8 15     SPACE eurjchem-207 8 16 to to PART eurjchem-207 8 17     SPACE eurjchem-207 8 18 treat treat VERB eurjchem-207 8 19     SPACE eurjchem-207 8 20 certain certain ADJ eurjchem-207 8 21     SPACE eurjchem-207 8 22 types type NOUN eurjchem-207 8 23     SPACE eurjchem-207 8 24 of of ADP eurjchem-207 8 25     SPACE eurjchem-207 8 26 cancer cancer NOUN eurjchem-207 8 27     SPACE eurjchem-207 8 28 that that PRON eurjchem-207 8 29     SPACE eurjchem-207 8 30 belongs belong VERB eurjchem-207 8 31     SPACE eurjchem-207 8 32 to to ADP eurjchem-207 8 33     SPACE eurjchem-207 8 34 a a DET eurjchem-207 8 35     SPACE eurjchem-207 8 36 new new ADJ eurjchem-207 8 37     SPACE eurjchem-207 8 38 class class NOUN eurjchem-207 8 39     SPACE eurjchem-207 8 40 of of ADP eurjchem-207 8 41     SPACE eurjchem-207 8 42 agents agent NOUN eurjchem-207 8 43     SPACE eurjchem-207 8 44 that that SCONJ eurjchem-207 8 45     SPACE eurjchem-207 8 46 act act NOUN eurjchem-207 8 47     SPACE eurjchem-207 8 48 by by ADP eurjchem-207 8 49     SPACE eurjchem-207 8 50 inhibiting inhibit VERB eurjchem-207 8 51     SPACE eurjchem-207 8 52 particular particular ADJ eurjchem-207 8 53     SPACE eurjchem-207 8 54 tyrosine tyrosine NOUN eurjchem-207 8 55     SPACE eurjchem-207 8 56 kinase kinase NOUN eurjchem-207 8 57     SPACE eurjchem-207 8 58 enzymes enzyme NOUN eurjchem-207 8 59 , , PUNCT eurjchem-207 8 60     SPACE eurjchem-207 8 61 instead instead ADV eurjchem-207 8 62     SPACE eurjchem-207 8 63 of of ADP eurjchem-207 8 64     SPACE eurjchem-207 8 65 non‐ non‐ ADV eurjchem-207 8 66 specifically specifically ADV eurjchem-207 8 67     SPACE eurjchem-207 8 68 inhibiting inhibit VERB eurjchem-207 8 69     SPACE eurjchem-207 8 70 rapidly rapidly ADV eurjchem-207 8 71     SPACE eurjchem-207 8 72 dividing divide VERB eurjchem-207 8 73     SPACE eurjchem-207 8 74 cells cell NOUN eurjchem-207 8 75     SPACE eurjchem-207 9 1 [ [ X eurjchem-207 9 2 6 6 NUM eurjchem-207 9 3 ] ] PUNCT eurjchem-207 9 4 . . PUNCT eurjchem-207 9 5     SPACE eurjchem-207 9 6 pyridylmethyl‐ pyridylmethyl‐ PROPN eurjchem-207 9 7 containing contain VERB eurjchem-207 9 8     SPACE eurjchem-207 9 9 benzanilides benzanilide NOUN eurjchem-207 9 10     SPACE eurjchem-207 9 11 are be AUX eurjchem-207 9 12     SPACE eurjchem-207 9 13 vascular vascular ADJ eurjchem-207 9 14     SPACE eurjchem-207 9 15 endothelial endothelial NOUN eurjchem-207 9 16     SPACE eurjchem-207 9 17 growth growth NOUN eurjchem-207 9 18     SPACE eurjchem-207 9 19 factor factor NOUN eurjchem-207 9 20     SPACE eurjchem-207 9 21 receptors receptor NOUN eurjchem-207 9 22     SPACE eurjchem-207 9 23 and and CCONJ eurjchem-207 9 24     SPACE eurjchem-207 9 25 tyrosine tyrosine NOUN eurjchem-207 9 26     SPACE eurjchem-207 9 27 kinase kinase NOUN eurjchem-207 9 28     SPACE eurjchem-207 9 29 inhibitors inhibitor NOUN eurjchem-207 9 30     SPACE eurjchem-207 9 31 [ [ X eurjchem-207 9 32 7 7 NUM eurjchem-207 9 33 ] ] PUNCT eurjchem-207 9 34 . . PUNCT eurjchem-207 9 35     SPACE eurjchem-207 9 36 the the DET eurjchem-207 9 37     SPACE eurjchem-207 9 38 title title NOUN eurjchem-207 9 39     SPACE eurjchem-207 9 40 compound compound NOUN eurjchem-207 9 41     SPACE eurjchem-207 9 42 ( ( PUNCT eurjchem-207 9 43 i i NOUN eurjchem-207 9 44 ) ) PUNCT eurjchem-207 9 45 , , PUNCT eurjchem-207 9 46     SPACE eurjchem-207 9 47 ( ( PUNCT eurjchem-207 9 48 figure figure NOUN eurjchem-207 9 49     SPACE eurjchem-207 9 50 1 1 NUM eurjchem-207 9 51 ) ) PUNCT eurjchem-207 9 52     SPACE eurjchem-207 9 53 was be AUX eurjchem-207 9 54     SPACE eurjchem-207 9 55 synthesized synthesize VERB eurjchem-207 9 56     SPACE eurjchem-207 9 57 in in ADP eurjchem-207 9 58     SPACE eurjchem-207 9 59 order order NOUN eurjchem-207 9 60     SPACE eurjchem-207 9 61 to to PART eurjchem-207 9 62     SPACE eurjchem-207 9 63 investigate investigate VERB eurjchem-207 9 64     SPACE eurjchem-207 9 65 the the DET eurjchem-207 9 66     SPACE eurjchem-207 9 67 combined combine VERB eurjchem-207 9 68     SPACE eurjchem-207 9 69 effects effect NOUN eurjchem-207 9 70     SPACE eurjchem-207 9 71 on on ADP eurjchem-207 9 72     SPACE eurjchem-207 9 73 biological biological ADJ eurjchem-207 9 74     SPACE eurjchem-207 9 75 activities activity NOUN eurjchem-207 9 76     SPACE eurjchem-207 9 77 of of ADP eurjchem-207 9 78     SPACE eurjchem-207 9 79 the the DET eurjchem-207 9 80     SPACE eurjchem-207 9 81 benzanilide benzanilide NOUN eurjchem-207 9 82     SPACE eurjchem-207 9 83 and and CCONJ eurjchem-207 9 84     SPACE eurjchem-207 9 85 other other ADJ eurjchem-207 9 86     SPACE eurjchem-207 9 87 heterocycles heterocycle NOUN eurjchem-207 9 88     SPACE eurjchem-207 9 89 combined combine VERB eurjchem-207 9 90     SPACE eurjchem-207 9 91 in in ADP eurjchem-207 9 92     SPACE eurjchem-207 9 93 a a DET eurjchem-207 9 94     SPACE eurjchem-207 9 95 single single ADJ eurjchem-207 9 96     SPACE eurjchem-207 9 97 structural structural ADJ eurjchem-207 9 98     SPACE eurjchem-207 9 99 unit unit NOUN eurjchem-207 9 100 . . PUNCT eurjchem-207 9 101         SPACE eurjchem-207 9 102 figure figure NOUN eurjchem-207 9 103     SPACE eurjchem-207 9 104 1 1 NUM eurjchem-207 9 105 . . PUNCT eurjchem-207 9 106     SPACE eurjchem-207 9 107 molecular molecular ADJ eurjchem-207 9 108     SPACE eurjchem-207 9 109 structure structure NOUN eurjchem-207 9 110     SPACE eurjchem-207 9 111 of of ADP eurjchem-207 9 112     SPACE eurjchem-207 9 113 the the DET eurjchem-207 9 114     SPACE eurjchem-207 9 115 title title NOUN eurjchem-207 9 116     SPACE eurjchem-207 9 117 compound compound NOUN eurjchem-207 9 118     SPACE eurjchem-207 9 119 with with ADP eurjchem-207 9 120     SPACE eurjchem-207 9 121 the the DET eurjchem-207 9 122     SPACE eurjchem-207 9 123 atom‐ atom‐ NOUN eurjchem-207 9 124 numbering numbering NOUN eurjchem-207 9 125     SPACE eurjchem-207 9 126 scheme scheme NOUN eurjchem-207 9 127 . . PUNCT eurjchem-207 9 128     SPACE eurjchem-207 9 129 displacement displacement NOUN eurjchem-207 9 130     SPACE eurjchem-207 9 131 ellipsoids ellipsoid NOUN eurjchem-207 9 132     SPACE eurjchem-207 9 133 are be AUX eurjchem-207 9 134     SPACE eurjchem-207 9 135 plotted plot VERB eurjchem-207 9 136     SPACE eurjchem-207 9 137 at at ADP eurjchem-207 9 138     SPACE eurjchem-207 9 139 50 50 NUM eurjchem-207 9 140 % % NOUN eurjchem-207 9 141     SPACE eurjchem-207 9 142 probability probability NOUN eurjchem-207 9 143     SPACE eurjchem-207 9 144 level level NOUN eurjchem-207 9 145 . . PUNCT eurjchem-207 9 146         SPACE eurjchem-207 10 1 2 2 NUM eurjchem-207 10 2 . . PUNCT eurjchem-207 10 3     SPACE eurjchem-207 10 4 experimental experimental ADJ eurjchem-207 10 5         SPACE eurjchem-207 10 6 2.1 2.1 NUM eurjchem-207 10 7 . . PUNCT eurjchem-207 10 8     SPACE eurjchem-207 10 9 instrumentations instrumentation NOUN eurjchem-207 10 10         SPACE eurjchem-207 10 11 melting melting NOUN eurjchem-207 10 12     SPACE eurjchem-207 10 13 points point NOUN eurjchem-207 10 14     SPACE eurjchem-207 10 15 were be AUX eurjchem-207 10 16     SPACE eurjchem-207 10 17 recorded record VERB eurjchem-207 10 18     SPACE eurjchem-207 10 19 using use VERB eurjchem-207 10 20     SPACE eurjchem-207 10 21 a a DET eurjchem-207 10 22     SPACE eurjchem-207 10 23 digital digital ADJ eurjchem-207 10 24     SPACE eurjchem-207 10 25 gallenkamp gallenkamp NOUN eurjchem-207 10 26     SPACE eurjchem-207 10 27 ( ( PUNCT eurjchem-207 10 28 sanyo sanyo PROPN eurjchem-207 10 29 ) ) PUNCT eurjchem-207 10 30     SPACE eurjchem-207 10 31 model model NOUN eurjchem-207 10 32     SPACE eurjchem-207 10 33 mpd.bm mpd.bm NOUN eurjchem-207 10 34     SPACE eurjchem-207 10 35 3.5 3.5 NUM eurjchem-207 10 36     SPACE eurjchem-207 10 37 apparatus apparatus NOUN eurjchem-207 10 38     SPACE eurjchem-207 10 39 and and CCONJ eurjchem-207 10 40     SPACE eurjchem-207 10 41 are be AUX eurjchem-207 10 42     SPACE eurjchem-207 10 43 uncorrected uncorrecte VERB eurjchem-207 10 44 . . PUNCT eurjchem-207 10 45     SPACE eurjchem-207 10 46 1h 1h NUM eurjchem-207 10 47     SPACE eurjchem-207 10 48 nmr nmr NOUN eurjchem-207 10 49     SPACE eurjchem-207 10 50 spectra spectra NOUN eurjchem-207 10 51     SPACE eurjchem-207 10 52 were be AUX eurjchem-207 10 53     SPACE eurjchem-207 10 54 determined determine VERB eurjchem-207 10 55     SPACE eurjchem-207 10 56 in in ADP eurjchem-207 10 57     SPACE eurjchem-207 10 58 cdcl3 cdcl3 NOUN eurjchem-207 10 59     SPACE eurjchem-207 10 60 at at ADP eurjchem-207 10 61     SPACE eurjchem-207 10 62 300 300 NUM eurjchem-207 10 63     SPACE eurjchem-207 10 64 mhz mhz NOUN eurjchem-207 10 65     SPACE eurjchem-207 10 66 using use VERB eurjchem-207 10 67     SPACE eurjchem-207 10 68 a a DET eurjchem-207 10 69     SPACE eurjchem-207 10 70 bruker bruker NOUN eurjchem-207 10 71     SPACE eurjchem-207 10 72 machine machine NOUN eurjchem-207 10 73 . . PUNCT eurjchem-207 10 74     SPACE eurjchem-207 10 75 ftir ftir PROPN eurjchem-207 10 76     SPACE eurjchem-207 10 77 spectra spectra PROPN eurjchem-207 10 78     SPACE eurjchem-207 10 79 were be AUX eurjchem-207 10 80     SPACE eurjchem-207 10 81 recorded record VERB eurjchem-207 10 82     SPACE eurjchem-207 10 83 on on ADP eurjchem-207 10 84     SPACE eurjchem-207 10 85 an an DET eurjchem-207 10 86     SPACE eurjchem-207 10 87 fts fts X eurjchem-207 10 88     SPACE eurjchem-207 10 89 3000 3000 NUM eurjchem-207 10 90     SPACE eurjchem-207 10 91 mx mx NOUN eurjchem-207 10 92     SPACE eurjchem-207 10 93 spectrophotometer spectrophotometer NOUN eurjchem-207 10 94 . . PUNCT eurjchem-207 10 95     SPACE eurjchem-207 10 96 mass mass PROPN eurjchem-207 10 97     SPACE eurjchem-207 10 98 spectrometry spectrometry NOUN eurjchem-207 10 99     SPACE eurjchem-207 10 100 ( ( PUNCT eurjchem-207 10 101 ei ei PROPN eurjchem-207 10 102 , , PUNCT eurjchem-207 10 103     SPACE eurjchem-207 10 104 70 70 NUM eurjchem-207 10 105     SPACE eurjchem-207 10 106 ev ev NOUN eurjchem-207 10 107 ) ) PUNCT eurjchem-207 10 108     SPACE eurjchem-207 10 109 were be AUX eurjchem-207 10 110     SPACE eurjchem-207 10 111 conducted conduct VERB eurjchem-207 10 112     SPACE eurjchem-207 10 113 on on ADP eurjchem-207 10 114     SPACE eurjchem-207 10 115 a a DET eurjchem-207 10 116     SPACE eurjchem-207 10 117 mat mat NOUN eurjchem-207 10 118     SPACE eurjchem-207 10 119 312 312 NUM eurjchem-207 10 120     SPACE eurjchem-207 10 121 instrument instrument NOUN eurjchem-207 10 122 , , PUNCT eurjchem-207 10 123     SPACE eurjchem-207 10 124 and and CCONJ eurjchem-207 10 125     SPACE eurjchem-207 10 126 elemental elemental NOUN eurjchem-207 10 127     SPACE eurjchem-207 10 128 analyses analysis NOUN eurjchem-207 10 129     SPACE eurjchem-207 10 130 were be AUX eurjchem-207 10 131     SPACE eurjchem-207 10 132 conducted conduct VERB eurjchem-207 10 133     SPACE eurjchem-207 10 134 using use VERB eurjchem-207 10 135     SPACE eurjchem-207 10 136 a a DET eurjchem-207 10 137     SPACE eurjchem-207 10 138 leco‐183 leco‐183 ADJ eurjchem-207 10 139     SPACE eurjchem-207 10 140 chns chns PROPN eurjchem-207 10 141     SPACE eurjchem-207 10 142 analyzer analyzer NOUN eurjchem-207 10 143 . . PUNCT eurjchem-207 10 144     SPACE eurjchem-207 10 145 crystallographic crystallographic ADJ eurjchem-207 10 146     SPACE eurjchem-207 10 147 data datum NOUN eurjchem-207 10 148     SPACE eurjchem-207 10 149 were be AUX eurjchem-207 10 150     SPACE eurjchem-207 10 151 collected collect VERB eurjchem-207 10 152     SPACE eurjchem-207 10 153 on on ADP eurjchem-207 10 154     SPACE eurjchem-207 10 155 a a DET eurjchem-207 10 156     SPACE eurjchem-207 10 157 bruker‐axs bruker‐axs PROPN eurjchem-207 10 158     SPACE eurjchem-207 10 159 smart smart ADJ eurjchem-207 10 160     SPACE eurjchem-207 10 161 apex apex NOUN eurjchem-207 10 162     SPACE eurjchem-207 10 163 ccd ccd PROPN eurjchem-207 10 164     SPACE eurjchem-207 10 165 diffractometer diffractometer NOUN eurjchem-207 10 166     SPACE eurjchem-207 10 167 using use VERB eurjchem-207 10 168     SPACE eurjchem-207 10 169 mok‐radiation mok‐radiation PROPN eurjchem-207 10 170 . . PUNCT eurjchem-207 10 171     SPACE eurjchem-207 11 1 the the DET eurjchem-207 11 2     SPACE eurjchem-207 11 3 crystal crystal NOUN eurjchem-207 11 4     SPACE eurjchem-207 11 5 structure structure NOUN eurjchem-207 11 6     SPACE eurjchem-207 11 7 was be AUX eurjchem-207 11 8     SPACE eurjchem-207 11 9 solved solve VERB eurjchem-207 11 10     SPACE eurjchem-207 11 11 by by ADP eurjchem-207 11 12     SPACE eurjchem-207 11 13 direct direct ADJ eurjchem-207 11 14     SPACE eurjchem-207 11 15 methods method NOUN eurjchem-207 11 16 . . PUNCT eurjchem-207 11 17     SPACE eurjchem-207 12 1 h‐atoms h‐atom NOUN eurjchem-207 12 2     SPACE eurjchem-207 12 3 were be AUX eurjchem-207 12 4     SPACE eurjchem-207 12 5 located locate VERB eurjchem-207 12 6     SPACE eurjchem-207 12 7 from from ADP eurjchem-207 12 8     SPACE eurjchem-207 12 9 difference difference NOUN eurjchem-207 12 10     SPACE eurjchem-207 12 11 fourier fourier NOUN eurjchem-207 12 12     SPACE eurjchem-207 12 13 maps map NOUN eurjchem-207 12 14     SPACE eurjchem-207 12 15 and and CCONJ eurjchem-207 12 16     SPACE eurjchem-207 12 17 then then ADV eurjchem-207 12 18     SPACE eurjchem-207 12 19 refined refine VERB eurjchem-207 12 20     SPACE eurjchem-207 12 21 at at ADP eurjchem-207 12 22     SPACE eurjchem-207 12 23 idealized idealize VERB eurjchem-207 12 24     SPACE eurjchem-207 12 25 positions position NOUN eurjchem-207 12 26     SPACE eurjchem-207 12 27 with with ADP eurjchem-207 12 28     SPACE eurjchem-207 12 29 the the DET eurjchem-207 12 30     SPACE eurjchem-207 12 31 riding ride VERB eurjchem-207 12 32     SPACE eurjchem-207 12 33 model model NOUN eurjchem-207 12 34 . . PUNCT eurjchem-207 12 35     SPACE eurjchem-207 13 1 details detail NOUN eurjchem-207 13 2     SPACE eurjchem-207 13 3 on on ADP eurjchem-207 13 4     SPACE eurjchem-207 13 5 data datum NOUN eurjchem-207 13 6     SPACE eurjchem-207 13 7 collection collection NOUN eurjchem-207 13 8     SPACE eurjchem-207 13 9 and and CCONJ eurjchem-207 13 10     SPACE eurjchem-207 13 11 refinement refinement NOUN eurjchem-207 13 12     SPACE eurjchem-207 13 13 are be AUX eurjchem-207 13 14     SPACE eurjchem-207 13 15 given give VERB eurjchem-207 13 16     SPACE eurjchem-207 13 17 in in ADP eurjchem-207 13 18     SPACE eurjchem-207 13 19 table table NOUN eurjchem-207 13 20     SPACE eurjchem-207 13 21 1 1 NUM eurjchem-207 13 22 . . PUNCT eurjchem-207 13 23         SPACE eurjchem-207 13 24 2.2 2.2 NUM eurjchem-207 13 25 . . PUNCT eurjchem-207 13 26     SPACE eurjchem-207 13 27 synthesis synthesis NOUN eurjchem-207 13 28         SPACE eurjchem-207 13 29 ethyl ethyl PROPN eurjchem-207 13 30     SPACE eurjchem-207 14 1 4‐aminobenzoate 4‐aminobenzoate PRON eurjchem-207 14 2     SPACE eurjchem-207 14 3 was be AUX eurjchem-207 14 4     SPACE eurjchem-207 14 5 prepared prepare VERB eurjchem-207 14 6     SPACE eurjchem-207 14 7 from from ADP eurjchem-207 14 8     SPACE eurjchem-207 14 9 commercial commercial ADJ eurjchem-207 14 10               SPACE eurjchem-207 14 11 4‐aminobenzoic 4‐aminobenzoic ADJ eurjchem-207 14 12     SPACE eurjchem-207 14 13 acid acid NOUN eurjchem-207 14 14     SPACE eurjchem-207 14 15 by by ADP eurjchem-207 14 16     SPACE eurjchem-207 14 17 refluxing refluxing NOUN eurjchem-207 14 18     SPACE eurjchem-207 14 19 with with ADP eurjchem-207 14 20     SPACE eurjchem-207 14 21 dry dry ADJ eurjchem-207 14 22     SPACE eurjchem-207 14 23 ethanol ethanol NOUN eurjchem-207 14 24     SPACE eurjchem-207 14 25 for for ADP eurjchem-207 14 26     SPACE eurjchem-207 14 27 20 20 NUM eurjchem-207 14 28     SPACE eurjchem-207 14 29 h. h. NOUN eurjchem-207 14 30     SPACE eurjchem-207 14 31 a a DET eurjchem-207 14 32     SPACE eurjchem-207 14 33 solution solution NOUN eurjchem-207 14 34     SPACE eurjchem-207 14 35 of of ADP eurjchem-207 14 36     SPACE eurjchem-207 14 37 4‐chlorobenzoyl 4‐chlorobenzoyl NOUN eurjchem-207 14 38     SPACE eurjchem-207 14 39 chloride chloride NOUN eurjchem-207 14 40     SPACE eurjchem-207 14 41 ( ( PUNCT eurjchem-207 14 42 10 10 NUM eurjchem-207 14 43     SPACE eurjchem-207 14 44 mmol mmol NOUN eurjchem-207 14 45 ) ) PUNCT eurjchem-207 14 46     SPACE eurjchem-207 14 47 in in ADP eurjchem-207 14 48     SPACE eurjchem-207 14 49 dry dry ADJ eurjchem-207 14 50     SPACE eurjchem-207 14 51 tetrahydrofuran tetrahydrofuran NOUN eurjchem-207 14 52     SPACE eurjchem-207 14 53 ( ( PUNCT eurjchem-207 14 54 thf thf NOUN eurjchem-207 14 55 ) ) PUNCT eurjchem-207 14 56     SPACE eurjchem-207 14 57 ( ( PUNCT eurjchem-207 14 58 25 25 NUM eurjchem-207 14 59     SPACE eurjchem-207 14 60 ml ml NOUN eurjchem-207 14 61 ) ) PUNCT eurjchem-207 14 62     SPACE eurjchem-207 14 63 was be AUX eurjchem-207 14 64     SPACE eurjchem-207 14 65 added add VERB eurjchem-207 14 66     SPACE eurjchem-207 14 67 dropwise dropwise NOUN eurjchem-207 14 68     SPACE eurjchem-207 14 69 to to ADP eurjchem-207 14 70     SPACE eurjchem-207 14 71 a a DET eurjchem-207 14 72     SPACE eurjchem-207 14 73 solution solution NOUN eurjchem-207 14 74     SPACE eurjchem-207 14 75 of of ADP eurjchem-207 14 76     SPACE eurjchem-207 14 77 ethyl ethyl PROPN eurjchem-207 14 78     SPACE eurjchem-207 15 1 4‐aminobenzoate 4‐aminobenzoate PRON eurjchem-207 15 2     SPACE eurjchem-207 15 3 ( ( PUNCT eurjchem-207 15 4 10 10 NUM eurjchem-207 15 5     SPACE eurjchem-207 15 6 mmol mmol NOUN eurjchem-207 15 7 ) ) PUNCT eurjchem-207 15 8     SPACE eurjchem-207 15 9 in in ADP eurjchem-207 15 10     SPACE eurjchem-207 15 11 dry dry ADJ eurjchem-207 15 12     SPACE eurjchem-207 15 13 thf thf NOUN eurjchem-207 15 14     SPACE eurjchem-207 15 15 ( ( PUNCT eurjchem-207 15 16 15 15 NUM eurjchem-207 15 17     SPACE eurjchem-207 15 18 ml ml NOUN eurjchem-207 15 19 ) ) PUNCT eurjchem-207 15 20     SPACE eurjchem-207 15 21 under under ADP eurjchem-207 15 22     SPACE eurjchem-207 15 23 a a DET eurjchem-207 15 24     SPACE eurjchem-207 15 25 nitrogen nitrogen NOUN eurjchem-207 15 26     SPACE eurjchem-207 15 27 atmosphere atmosphere NOUN eurjchem-207 15 28     SPACE eurjchem-207 15 29 at at ADP eurjchem-207 15 30     SPACE eurjchem-207 15 31 reflux reflux NOUN eurjchem-207 15 32     SPACE eurjchem-207 15 33 for for ADP eurjchem-207 15 34     SPACE eurjchem-207 15 35 4 4 NUM eurjchem-207 15 36     SPACE eurjchem-207 15 37 h. h. NOUN eurjchem-207 15 38     SPACE eurjchem-207 15 39 the the DET eurjchem-207 15 40     SPACE eurjchem-207 15 41 reaction reaction NOUN eurjchem-207 15 42     SPACE eurjchem-207 15 43 mixture mixture NOUN eurjchem-207 15 44     SPACE eurjchem-207 15 45 was be AUX eurjchem-207 15 46     SPACE eurjchem-207 15 47 poured pour VERB eurjchem-207 15 48     SPACE eurjchem-207 15 49 into into ADP eurjchem-207 15 50     SPACE eurjchem-207 15 51 five five NUM eurjchem-207 15 52     SPACE eurjchem-207 15 53 times time NOUN eurjchem-207 15 54     SPACE eurjchem-207 15 55 its its PRON eurjchem-207 15 56     SPACE eurjchem-207 15 57 volume volume NOUN eurjchem-207 15 58     SPACE eurjchem-207 15 59 of of ADP eurjchem-207 15 60     SPACE eurjchem-207 15 61 cold cold ADJ eurjchem-207 15 62     SPACE eurjchem-207 15 63 water water NOUN eurjchem-207 15 64     SPACE eurjchem-207 15 65 when when SCONJ eurjchem-207 15 66     SPACE eurjchem-207 15 67 the the DET eurjchem-207 15 68     SPACE eurjchem-207 15 69 amide amide NOUN eurjchem-207 15 70     SPACE eurjchem-207 15 71 was be AUX eurjchem-207 15 72     SPACE eurjchem-207 15 73 precipitated precipitate VERB eurjchem-207 15 74     SPACE eurjchem-207 15 75 as as ADP eurjchem-207 15 76     SPACE eurjchem-207 15 77 a a DET eurjchem-207 15 78     SPACE eurjchem-207 15 79 solid solid ADJ eurjchem-207 15 80 . . PUNCT eurjchem-207 15 81     SPACE eurjchem-207 15 82 recrystallization recrystallization NOUN eurjchem-207 15 83     SPACE eurjchem-207 15 84 from from ADP eurjchem-207 15 85     SPACE eurjchem-207 15 86 ethanol ethanol NOUN eurjchem-207 15 87     SPACE eurjchem-207 15 88 afforded afford VERB eurjchem-207 15 89     SPACE eurjchem-207 15 90 the the DET eurjchem-207 15 91     SPACE eurjchem-207 15 92 title title NOUN eurjchem-207 15 93     SPACE eurjchem-207 15 94 compound compound NOUN eurjchem-207 15 95     SPACE eurjchem-207 15 96 as as ADP eurjchem-207 15 97     SPACE eurjchem-207 15 98 colorless colorless ADJ eurjchem-207 15 99     SPACE eurjchem-207 15 100 crystals crystal NOUN eurjchem-207 15 101 . . PUNCT eurjchem-207 15 102     SPACE eurjchem-207 15 103 yield yield NOUN eurjchem-207 15 104 : : PUNCT eurjchem-207 15 105     SPACE eurjchem-207 15 106 81 81 NUM eurjchem-207 15 107 % % NOUN eurjchem-207 15 108 . . PUNCT eurjchem-207 15 109     SPACE eurjchem-207 16 1 m.p m.p PROPN eurjchem-207 16 2 . . PROPN eurjchem-207 16 3 : : PUNCT eurjchem-207 16 4     SPACE eurjchem-207 16 5 156‐158 156‐158 NOUN eurjchem-207 16 6     SPACE eurjchem-207 16 7 oc oc PROPN eurjchem-207 16 8 . . PUNCT eurjchem-207 16 9     SPACE eurjchem-207 16 10 ir ir VERB eurjchem-207 16 11     SPACE eurjchem-207 16 12 ( ( PUNCT eurjchem-207 16 13 kbr kbr PROPN eurjchem-207 16 14 , , PUNCT eurjchem-207 16 15     SPACE eurjchem-207 16 16 cm‐1 cm‐1 NOUN eurjchem-207 16 17 ): ): PUNCT eurjchem-207 16 18     SPACE eurjchem-207 16 19 3300 3300 NUM eurjchem-207 16 20     SPACE eurjchem-207 16 21 ν(nh ν(nh NOUN eurjchem-207 16 22 ) ) PUNCT eurjchem-207 16 23 , , PUNCT eurjchem-207 16 24     SPACE eurjchem-207 16 25 1721 1721 NUM eurjchem-207 16 26     SPACE eurjchem-207 16 27 ν(ester ν(ester NOUN eurjchem-207 16 28     SPACE eurjchem-207 16 29 c c NOUN eurjchem-207 16 30 = = NOUN eurjchem-207 16 31 o o NOUN eurjchem-207 16 32 ) ) PUNCT eurjchem-207 16 33 , , PUNCT eurjchem-207 16 34     SPACE eurjchem-207 16 35 1665 1665 NUM eurjchem-207 16 36     SPACE eurjchem-207 16 37 ν(c ν(c PROPN eurjchem-207 16 38 = = SYM eurjchem-207 16 39 o o PROPN eurjchem-207 16 40 , , PUNCT eurjchem-207 16 41     SPACE eurjchem-207 16 42 amide amide NOUN eurjchem-207 16 43 ) ) PUNCT eurjchem-207 16 44 , , PUNCT eurjchem-207 16 45     SPACE eurjchem-207 16 46 1290 1290 NUM eurjchem-207 16 47     SPACE eurjchem-207 16 48 ν(c‐o ν(c‐o PROPN eurjchem-207 16 49 ) ) PUNCT eurjchem-207 16 50 , , PUNCT eurjchem-207 16 51     SPACE eurjchem-207 16 52 1154 1154 NUM eurjchem-207 16 53     SPACE eurjchem-207 16 54 ν(c−n ν(c−n NUM eurjchem-207 16 55 ) ) PUNCT eurjchem-207 16 56 , , PUNCT eurjchem-207 16 57     SPACE eurjchem-207 16 58 1593 1593 NUM eurjchem-207 16 59     SPACE eurjchem-207 16 60 ν(arom ν(arom NOUN eurjchem-207 16 61 . . PUNCT eurjchem-207 16 62 ) ) PUNCT eurjchem-207 16 63 . . PUNCT eurjchem-207 16 64     SPACE eurjchem-207 17 1 1h 1h NUM eurjchem-207 17 2     SPACE eurjchem-207 17 3 nmr nmr NOUN eurjchem-207 17 4     SPACE eurjchem-207 17 5 ( ( PUNCT eurjchem-207 17 6   NUM eurjchem-207 17 7 , , PUNCT eurjchem-207 17 8     SPACE eurjchem-207 17 9 ppm ppm NOUN eurjchem-207 17 10 ): ): PUNCT eurjchem-207 17 11     SPACE eurjchem-207 17 12 1.94 1.94 NUM eurjchem-207 17 13     SPACE eurjchem-207 17 14 ( ( PUNCT eurjchem-207 17 15 t t PROPN eurjchem-207 17 16 , , PUNCT eurjchem-207 17 17     SPACE eurjchem-207 17 18 3h 3h NUM eurjchem-207 17 19 , , PUNCT eurjchem-207 17 20     SPACE eurjchem-207 17 21 ch3 ch3 PROPN eurjchem-207 17 22 ) ) PUNCT eurjchem-207 17 23 , , PUNCT eurjchem-207 17 24     SPACE eurjchem-207 17 25 3.44 3.44 NUM eurjchem-207 17 26     SPACE eurjchem-207 17 27 ( ( PUNCT eurjchem-207 17 28 q q NOUN eurjchem-207 17 29 , , PUNCT eurjchem-207 17 30     SPACE eurjchem-207 17 31 2h 2h NUM eurjchem-207 17 32 , , PUNCT eurjchem-207 17 33     SPACE eurjchem-207 17 34 ch2 ch2 NOUN eurjchem-207 17 35 ) ) PUNCT eurjchem-207 17 36 , , PUNCT eurjchem-207 17 37     SPACE eurjchem-207 17 38 6.62‐7.16 6.62‐7.16 NOUN eurjchem-207 17 39     SPACE eurjchem-207 17 40 ( ( PUNCT eurjchem-207 17 41 m m PROPN eurjchem-207 17 42 , , PUNCT eurjchem-207 17 43     SPACE eurjchem-207 17 44 10h 10h NUM eurjchem-207 17 45 , , PUNCT eurjchem-207 17 46     SPACE eurjchem-207 17 47 ar ar NOUN eurjchem-207 17 48 ) ) PUNCT eurjchem-207 17 49 , , PUNCT eurjchem-207 17 50     SPACE eurjchem-207 17 51 9.04 9.04 NUM eurjchem-207 17 52     SPACE eurjchem-207 17 53 ( ( PUNCT eurjchem-207 17 54 s s PROPN eurjchem-207 17 55 , , PUNCT eurjchem-207 17 56     SPACE eurjchem-207 17 57 1h 1h NUM eurjchem-207 17 58 , , PUNCT eurjchem-207 17 59     SPACE eurjchem-207 17 60 broad broad ADJ eurjchem-207 17 61 , , PUNCT eurjchem-207 17 62     SPACE eurjchem-207 17 63 nh nh PROPN eurjchem-207 17 64 ) ) PUNCT eurjchem-207 17 65 . . PUNCT eurjchem-207 17 66     SPACE eurjchem-207 18 1 ei ei PROPN eurjchem-207 18 2     SPACE eurjchem-207 18 3 ms ms PROPN eurjchem-207 18 4     SPACE eurjchem-207 18 5 ( ( PUNCT eurjchem-207 18 6 m m PROPN eurjchem-207 18 7 / / SYM eurjchem-207 18 8 z z NOUN eurjchem-207 18 9 ): ): PUNCT eurjchem-207 18 10     SPACE eurjchem-207 18 11 305 305 NUM eurjchem-207 18 12 , , PUNCT eurjchem-207 18 13     SPACE eurjchem-207 18 14 303 303 NUM eurjchem-207 18 15     SPACE eurjchem-207 18 16 ( ( PUNCT eurjchem-207 18 17 m+ m+ NUM eurjchem-207 18 18 ) ) PUNCT eurjchem-207 18 19 , , PUNCT eurjchem-207 18 20     SPACE eurjchem-207 18 21 138.9 138.9 NUM eurjchem-207 18 22     SPACE eurjchem-207 18 23 ( ( PUNCT eurjchem-207 18 24 100 100 NUM eurjchem-207 18 25 % % NOUN eurjchem-207 18 26 ) ) PUNCT eurjchem-207 18 27 . . PUNCT eurjchem-207 18 28     SPACE eurjchem-207 19 1 anal anal ADJ eurjchem-207 19 2 . . PUNCT eurjchem-207 19 3     SPACE eurjchem-207 19 4 calcd calcd NOUN eurjchem-207 19 5 . . PUNCT eurjchem-207 19 6     SPACE eurjchem-207 19 7 for for ADP eurjchem-207 19 8     SPACE eurjchem-207 19 9 290 290 NUM eurjchem-207 19 10     SPACE eurjchem-207 19 11 saeed saeed PROPN eurjchem-207 19 12     SPACE eurjchem-207 19 13 et et PROPN eurjchem-207 19 14     SPACE eurjchem-207 19 15 al al PROPN eurjchem-207 19 16 . . PROPN eurjchem-207 19 17     SPACE eurjchem-207 19 18 / / SYM eurjchem-207 19 19     SPACE eurjchem-207 19 20 european european ADJ eurjchem-207 19 21     SPACE eurjchem-207 19 22 journal journal NOUN eurjchem-207 19 23     SPACE eurjchem-207 19 24 of of ADP eurjchem-207 19 25     SPACE eurjchem-207 19 26 chemistry chemistry NOUN eurjchem-207 19 27     SPACE eurjchem-207 19 28 1 1 NUM eurjchem-207 19 29     SPACE eurjchem-207 19 30 ( ( PUNCT eurjchem-207 19 31 4 4 NUM eurjchem-207 19 32 ) ) PUNCT eurjchem-207 19 33     SPACE eurjchem-207 19 34 ( ( PUNCT eurjchem-207 19 35 2010 2010 NUM eurjchem-207 19 36 ) ) PUNCT eurjchem-207 19 37     SPACE eurjchem-207 19 38 289­290 289­290 NUM eurjchem-207 19 39         SPACE eurjchem-207 19 40 c16h14clno3 c16h14clno3 NOUN eurjchem-207 19 41 , , PUNCT eurjchem-207 19 42     SPACE eurjchem-207 19 43 c c NOUN eurjchem-207 19 44 , , PUNCT eurjchem-207 19 45     SPACE eurjchem-207 19 46 63.27 63.27 NUM eurjchem-207 19 47 ; ; PUNCT eurjchem-207 19 48     SPACE eurjchem-207 19 49 h h NOUN eurjchem-207 19 50 , , PUNCT eurjchem-207 19 51     SPACE eurjchem-207 19 52 4.65 4.65 NUM eurjchem-207 19 53 ; ; PUNCT eurjchem-207 19 54     SPACE eurjchem-207 19 55 n n CCONJ eurjchem-207 19 56 , , PUNCT eurjchem-207 19 57     SPACE eurjchem-207 19 58 4.61 4.61 NUM eurjchem-207 19 59 . . PUNCT eurjchem-207 19 60     SPACE eurjchem-207 19 61 found find VERB eurjchem-207 19 62     SPACE eurjchem-207 19 63 c c NOUN eurjchem-207 19 64 , , PUNCT eurjchem-207 19 65     SPACE eurjchem-207 19 66 63.34 63.34 NUM eurjchem-207 19 67 ; ; PUNCT eurjchem-207 19 68     SPACE eurjchem-207 19 69 h h NOUN eurjchem-207 19 70 , , PUNCT eurjchem-207 19 71     SPACE eurjchem-207 19 72 4.56 4.56 NUM eurjchem-207 19 73 ; ; PUNCT eurjchem-207 19 74     SPACE eurjchem-207 19 75 n n CCONJ eurjchem-207 19 76 , , PUNCT eurjchem-207 19 77     SPACE eurjchem-207 19 78 4.68 4.68 NUM eurjchem-207 19 79 . . PUNCT eurjchem-207 19 80         SPACE eurjchem-207 19 81 table table NOUN eurjchem-207 19 82     SPACE eurjchem-207 19 83 1 1 NUM eurjchem-207 19 84 . . PUNCT eurjchem-207 19 85     SPACE eurjchem-207 19 86 crystal crystal NOUN eurjchem-207 19 87     SPACE eurjchem-207 19 88 and and CCONJ eurjchem-207 19 89     SPACE eurjchem-207 19 90 experimental experimental ADJ eurjchem-207 19 91     SPACE eurjchem-207 19 92 data datum NOUN eurjchem-207 19 93     SPACE eurjchem-207 19 94 of of ADP eurjchem-207 19 95     SPACE eurjchem-207 19 96 the the DET eurjchem-207 19 97     SPACE eurjchem-207 19 98 title title NOUN eurjchem-207 19 99     SPACE eurjchem-207 19 100 compound compound NOUN eurjchem-207 19 101 . . PUNCT eurjchem-207 19 102     SPACE eurjchem-207 20 1 empirical empirical ADJ eurjchem-207 20 2     SPACE eurjchem-207 20 3 formula formula NOUN eurjchem-207 20 4       SPACE eurjchem-207 20 5 c16h14clno3 c16h14clno3 NOUN eurjchem-207 20 6     SPACE eurjchem-207 20 7 formula formula NOUN eurjchem-207 20 8     SPACE eurjchem-207 20 9 weight weight NOUN eurjchem-207 20 10       SPACE eurjchem-207 20 11 303.73 303.73 NUM eurjchem-207 20 12     SPACE eurjchem-207 20 13 temperature temperature NOUN eurjchem-207 20 14       SPACE eurjchem-207 20 15 120(2 120(2 NUM eurjchem-207 20 16 ) ) PUNCT eurjchem-207 20 17     SPACE eurjchem-207 20 18 k k NOUN eurjchem-207 20 19     SPACE eurjchem-207 20 20 wavelength wavelength NOUN eurjchem-207 20 21       SPACE eurjchem-207 20 22 0.71073 0.71073 NUM eurjchem-207 20 23     SPACE eurjchem-207 20 24 å å PROPN eurjchem-207 20 25     SPACE eurjchem-207 20 26 crystal crystal NOUN eurjchem-207 20 27     SPACE eurjchem-207 20 28 system system NOUN eurjchem-207 20 29       SPACE eurjchem-207 20 30 triclinic triclinic ADJ eurjchem-207 20 31     SPACE eurjchem-207 20 32 space space NOUN eurjchem-207 20 33     SPACE eurjchem-207 20 34 group group NOUN eurjchem-207 20 35       SPACE eurjchem-207 20 36 p‐1 p‐1 PROPN eurjchem-207 20 37 unit unit NOUN eurjchem-207 20 38     SPACE eurjchem-207 20 39 cell cell NOUN eurjchem-207 20 40     SPACE eurjchem-207 20 41 dimensions dimension NOUN eurjchem-207 20 42     SPACE eurjchem-207 20 43 a a DET eurjchem-207 20 44 = = NOUN eurjchem-207 20 45     SPACE eurjchem-207 20 46 5.2941(15 5.2941(15 NUM eurjchem-207 20 47 ) ) PUNCT eurjchem-207 20 48     SPACE eurjchem-207 21 1 å å PROPN eurjchem-207 21 2     SPACE eurjchem-207 21 3 b b NOUN eurjchem-207 21 4     SPACE eurjchem-207 21 5 = = NOUN eurjchem-207 21 6     SPACE eurjchem-207 21 7 8.157(2 8.157(2 NUM eurjchem-207 21 8 ) ) PUNCT eurjchem-207 21 9     SPACE eurjchem-207 22 1 å å PROPN eurjchem-207 22 2     SPACE eurjchem-207 22 3 c c NOUN eurjchem-207 22 4     SPACE eurjchem-207 22 5 = = NOUN eurjchem-207 22 6     SPACE eurjchem-207 22 7 16.238(4 16.238(4 NOUN eurjchem-207 22 8 ) ) PUNCT eurjchem-207 22 9     SPACE eurjchem-207 22 10 å å PROPN eurjchem-207 22 11     SPACE eurjchem-207 22 12 = = ADJ eurjchem-207 22 13     SPACE eurjchem-207 22 14 82.682(6 82.682(6 NOUN eurjchem-207 22 15 ) ) PUNCT eurjchem-207 22 16 ° ° ADP eurjchem-207 22 17     SPACE eurjchem-207 22 18 = = NOUN eurjchem-207 22 19     SPACE eurjchem-207 22 20 84.481(6 84.481(6 NUM eurjchem-207 22 21 ) ) PUNCT eurjchem-207 22 22 ° ° ADP eurjchem-207 22 23     SPACE eurjchem-207 22 24   NOUN eurjchem-207 22 25     SPACE eurjchem-207 22 26 = = NOUN eurjchem-207 22 27     SPACE eurjchem-207 22 28 80.100(6 80.100(6 NOUN eurjchem-207 22 29 ) ) PUNCT eurjchem-207 22 30 ° ° ADP eurjchem-207 22 31     SPACE eurjchem-207 22 32 volume volume NOUN eurjchem-207 22 33     SPACE eurjchem-207 22 34 683.2(3 683.2(3 NUM eurjchem-207 22 35 ) ) PUNCT eurjchem-207 22 36     SPACE eurjchem-207 22 37 å3 å3 PROPN eurjchem-207 22 38     SPACE eurjchem-207 22 39 z z PROPN eurjchem-207 22 40     SPACE eurjchem-207 22 41 2 2 NUM eurjchem-207 22 42 density density NOUN eurjchem-207 22 43     SPACE eurjchem-207 22 44 ( ( PUNCT eurjchem-207 22 45 calculated calculate VERB eurjchem-207 22 46 ) ) PUNCT eurjchem-207 22 47     SPACE eurjchem-207 22 48 1.477 1.477 NUM eurjchem-207 22 49     SPACE eurjchem-207 22 50 mg mg PROPN eurjchem-207 22 51 / / SYM eurjchem-207 22 52 m3 m3 PROPN eurjchem-207 22 53     SPACE eurjchem-207 22 54 f(000 f(000 NOUN eurjchem-207 22 55 ) ) PUNCT eurjchem-207 22 56     SPACE eurjchem-207 22 57 316 316 NUM eurjchem-207 22 58 crystal crystal NOUN eurjchem-207 22 59     SPACE eurjchem-207 22 60 size size NOUN eurjchem-207 22 61     SPACE eurjchem-207 22 62 0.38 0.38 NUM eurjchem-207 22 63     SPACE eurjchem-207 22 64 x x NOUN eurjchem-207 22 65     SPACE eurjchem-207 22 66 0.22 0.22 NUM eurjchem-207 22 67     SPACE eurjchem-207 22 68 x x NOUN eurjchem-207 22 69     SPACE eurjchem-207 22 70 0.17 0.17 NUM eurjchem-207 22 71     SPACE eurjchem-207 22 72 mm3 mm3 PROPN eurjchem-207 22 73     SPACE eurjchem-207 22 74 theta theta NOUN eurjchem-207 22 75     SPACE eurjchem-207 22 76 range range NOUN eurjchem-207 22 77     SPACE eurjchem-207 22 78 for for ADP eurjchem-207 22 79     SPACE eurjchem-207 22 80 data datum NOUN eurjchem-207 22 81     SPACE eurjchem-207 22 82 collection collection NOUN eurjchem-207 22 83     SPACE eurjchem-207 22 84 1.27 1.27 NUM eurjchem-207 22 85     SPACE eurjchem-207 22 86 to to ADP eurjchem-207 22 87     SPACE eurjchem-207 22 88 27.88 27.88 NUM eurjchem-207 22 89 ° ° NUM eurjchem-207 22 90     SPACE eurjchem-207 22 91 index index NOUN eurjchem-207 22 92     SPACE eurjchem-207 22 93 ranges range VERB eurjchem-207 22 94     SPACE eurjchem-207 22 95 ‐6 ‐6 NOUN eurjchem-207 22 96     SPACE eurjchem-207 22 97   NOUN eurjchem-207 22 98     SPACE eurjchem-207 22 99 h h NOUN eurjchem-207 22 100     SPACE eurjchem-207 22 101   NOUN eurjchem-207 22 102     SPACE eurjchem-207 22 103 6 6 NUM eurjchem-207 22 104     SPACE eurjchem-207 22 105 ‐10 ‐10 NOUN eurjchem-207 22 106     SPACE eurjchem-207 22 107   NOUN eurjchem-207 22 108     SPACE eurjchem-207 22 109 k k NOUN eurjchem-207 22 110     SPACE eurjchem-207 22 111   NOUN eurjchem-207 22 112     SPACE eurjchem-207 22 113 10 10 NUM eurjchem-207 22 114     SPACE eurjchem-207 22 115 ‐21 ‐21 NOUN eurjchem-207 22 116     SPACE eurjchem-207 22 117   NOUN eurjchem-207 22 118     SPACE eurjchem-207 22 119 l l NOUN eurjchem-207 22 120     SPACE eurjchem-207 22 121   NOUN eurjchem-207 22 122     SPACE eurjchem-207 22 123 20 20 NUM eurjchem-207 22 124     SPACE eurjchem-207 22 125 reflections reflection NOUN eurjchem-207 22 126     SPACE eurjchem-207 22 127 collected collect VERB eurjchem-207 22 128     SPACE eurjchem-207 22 129 5988 5988 NUM eurjchem-207 22 130     SPACE eurjchem-207 22 131 independent independent ADJ eurjchem-207 22 132     SPACE eurjchem-207 22 133 reflections reflection NOUN eurjchem-207 22 134     SPACE eurjchem-207 22 135 3221 3221 NUM eurjchem-207 22 136     SPACE eurjchem-207 23 1 [ [ X eurjchem-207 23 2 rint rint NOUN eurjchem-207 23 3     SPACE eurjchem-207 23 4 = = NOUN eurjchem-207 23 5     SPACE eurjchem-207 23 6 0.0585 0.0585 NUM eurjchem-207 23 7 ] ] SYM eurjchem-207 23 8     SPACE eurjchem-207 23 9 completeness completeness NOUN eurjchem-207 23 10     SPACE eurjchem-207 23 11 to to ADP eurjchem-207 23 12     SPACE eurjchem-207 23 13 theta theta VERB eurjchem-207 23 14     SPACE eurjchem-207 23 15 = = NOUN eurjchem-207 23 16     SPACE eurjchem-207 23 17 27.88 27.88 NUM eurjchem-207 23 18 ° ° NOUN eurjchem-207 23 19     SPACE eurjchem-207 23 20 99.1 99.1 NUM eurjchem-207 23 21     SPACE eurjchem-207 23 22 % % NOUN eurjchem-207 23 23       SPACE eurjchem-207 23 24 absorption absorption NOUN eurjchem-207 23 25     SPACE eurjchem-207 23 26 correction correction NOUN eurjchem-207 23 27     SPACE eurjchem-207 23 28 semi‐empirical semi‐empirical NOUN eurjchem-207 23 29     SPACE eurjchem-207 23 30 from from ADP eurjchem-207 23 31     SPACE eurjchem-207 23 32 equivalents equivalent NOUN eurjchem-207 23 33 max max PROPN eurjchem-207 23 34 . . PUNCT eurjchem-207 23 35     SPACE eurjchem-207 23 36 and and CCONJ eurjchem-207 23 37     SPACE eurjchem-207 23 38 min min PROPN eurjchem-207 23 39 . . PROPN eurjchem-207 23 40     SPACE eurjchem-207 23 41 transmission transmission NOUN eurjchem-207 23 42     SPACE eurjchem-207 23 43 0.9525 0.9525 NUM eurjchem-207 23 44     SPACE eurjchem-207 23 45 and and CCONJ eurjchem-207 23 46     SPACE eurjchem-207 23 47 0.8981 0.8981 NUM eurjchem-207 23 48     SPACE eurjchem-207 23 49 refinement refinement NOUN eurjchem-207 23 50     SPACE eurjchem-207 23 51 method method NOUN eurjchem-207 23 52     SPACE eurjchem-207 23 53 full‐matrix full‐matrix NOUN eurjchem-207 23 54     SPACE eurjchem-207 23 55 least‐squares least‐square NOUN eurjchem-207 23 56     SPACE eurjchem-207 23 57 on on ADP eurjchem-207 23 58     SPACE eurjchem-207 23 59 f2 f2 PROPN eurjchem-207 23 60 data datum NOUN eurjchem-207 23 61     SPACE eurjchem-207 23 62 / / SYM eurjchem-207 23 63     SPACE eurjchem-207 23 64 restraints restraint NOUN eurjchem-207 23 65     SPACE eurjchem-207 23 66 / / SYM eurjchem-207 23 67     SPACE eurjchem-207 23 68 parameters parameter NOUN eurjchem-207 23 69     SPACE eurjchem-207 23 70 3221 3221 NUM eurjchem-207 23 71     SPACE eurjchem-207 23 72 / / SYM eurjchem-207 23 73     SPACE eurjchem-207 23 74 0 0 NUM eurjchem-207 23 75     SPACE eurjchem-207 23 76 / / SYM eurjchem-207 23 77     SPACE eurjchem-207 23 78 190 190 NUM eurjchem-207 23 79     SPACE eurjchem-207 23 80 goodness‐of‐fit goodness‐of‐fit NOUN eurjchem-207 23 81     SPACE eurjchem-207 23 82 on on ADP eurjchem-207 23 83     SPACE eurjchem-207 23 84 f2 f2 PROPN eurjchem-207 23 85     SPACE eurjchem-207 23 86 0.990 0.990 NUM eurjchem-207 23 87     SPACE eurjchem-207 23 88 final final ADJ eurjchem-207 23 89     SPACE eurjchem-207 23 90 r r NOUN eurjchem-207 23 91     SPACE eurjchem-207 23 92 indices index NOUN eurjchem-207 23 93     SPACE eurjchem-207 24 1 [ [ X eurjchem-207 24 2 i i PRON eurjchem-207 24 3     SPACE eurjchem-207 24 4 > > X eurjchem-207 24 5     SPACE eurjchem-207 24 6 2σ(i 2σ(i NUM eurjchem-207 24 7 ) ) PUNCT eurjchem-207 24 8 ] ] PUNCT eurjchem-207 24 9     SPACE eurjchem-207 24 10 r1 r1 NOUN eurjchem-207 24 11 = = NOUN eurjchem-207 24 12     SPACE eurjchem-207 24 13 0.0538 0.0538 NUM eurjchem-207 24 14 , , PUNCT eurjchem-207 24 15     SPACE eurjchem-207 24 16 wr2 wr2 PROPN eurjchem-207 24 17     SPACE eurjchem-207 24 18 = = NOUN eurjchem-207 24 19     SPACE eurjchem-207 24 20 0.111 0.111 NUM eurjchem-207 24 21     SPACE eurjchem-207 24 22 r r NOUN eurjchem-207 24 23     SPACE eurjchem-207 24 24 indices index NOUN eurjchem-207 24 25     SPACE eurjchem-207 24 26 ( ( PUNCT eurjchem-207 24 27 all all DET eurjchem-207 24 28     SPACE eurjchem-207 24 29 data datum NOUN eurjchem-207 24 30 ) ) PUNCT eurjchem-207 24 31     SPACE eurjchem-207 24 32 r1 r1 NOUN eurjchem-207 24 33 = = SYM eurjchem-207 24 34     SPACE eurjchem-207 24 35 0.0846 0.0846 NUM eurjchem-207 24 36 , , PUNCT eurjchem-207 24 37     SPACE eurjchem-207 24 38 wr2 wr2 PROPN eurjchem-207 24 39     SPACE eurjchem-207 24 40 = = NOUN eurjchem-207 24 41     SPACE eurjchem-207 24 42 0.1208 0.1208 NUM eurjchem-207 24 43 largest large ADJ eurjchem-207 24 44     SPACE eurjchem-207 24 45 diff diff NOUN eurjchem-207 24 46 . . PUNCT eurjchem-207 24 47     SPACE eurjchem-207 24 48 peak peak NOUN eurjchem-207 24 49     SPACE eurjchem-207 24 50 and and CCONJ eurjchem-207 24 51     SPACE eurjchem-207 24 52 hole hole NOUN eurjchem-207 24 53     SPACE eurjchem-207 24 54 0.498 0.498 NUM eurjchem-207 24 55     SPACE eurjchem-207 24 56 and and CCONJ eurjchem-207 24 57     SPACE eurjchem-207 24 58 0.362 0.362 NUM eurjchem-207 24 59     SPACE eurjchem-207 24 60 e.å‐3 e.å‐3 PROPN eurjchem-207 24 61     SPACE eurjchem-207 24 62 ccdc ccdc NOUN eurjchem-207 24 63       SPACE eurjchem-207 24 64 679109 679109 NUM eurjchem-207 24 65           SPACE eurjchem-207 24 66 3 3 NUM eurjchem-207 24 67 . . PUNCT eurjchem-207 24 68     SPACE eurjchem-207 24 69 results result VERB eurjchem-207 24 70     SPACE eurjchem-207 24 71 and and CCONJ eurjchem-207 24 72     SPACE eurjchem-207 24 73 discussion discussion NOUN eurjchem-207 24 74         SPACE eurjchem-207 24 75 commercial commercial ADJ eurjchem-207 24 76     SPACE eurjchem-207 24 77 4‐aminobenzoic 4‐aminobenzoic ADJ eurjchem-207 24 78     SPACE eurjchem-207 24 79 acid acid NOUN eurjchem-207 24 80     SPACE eurjchem-207 24 81 was be AUX eurjchem-207 24 82     SPACE eurjchem-207 24 83 converted convert VERB eurjchem-207 24 84     SPACE eurjchem-207 24 85 into into ADP eurjchem-207 24 86     SPACE eurjchem-207 24 87 its its PRON eurjchem-207 24 88     SPACE eurjchem-207 24 89 ethyl ethyl NOUN eurjchem-207 24 90     SPACE eurjchem-207 24 91 ester ester NOUN eurjchem-207 24 92     SPACE eurjchem-207 24 93 by by ADP eurjchem-207 24 94     SPACE eurjchem-207 24 95 refluxing refluxing NOUN eurjchem-207 24 96     SPACE eurjchem-207 24 97 with with ADP eurjchem-207 24 98     SPACE eurjchem-207 24 99 dry dry ADJ eurjchem-207 24 100     SPACE eurjchem-207 24 101 ethanol ethanol NOUN eurjchem-207 24 102     SPACE eurjchem-207 24 103 according accord VERB eurjchem-207 24 104     SPACE eurjchem-207 24 105 to to ADP eurjchem-207 24 106     SPACE eurjchem-207 24 107 the the DET eurjchem-207 24 108     SPACE eurjchem-207 24 109 standard standard ADJ eurjchem-207 24 110     SPACE eurjchem-207 24 111 procedure procedure NOUN eurjchem-207 24 112 . . PUNCT eurjchem-207 24 113     SPACE eurjchem-207 25 1 treatment treatment NOUN eurjchem-207 25 2     SPACE eurjchem-207 25 3 of of ADP eurjchem-207 25 4     SPACE eurjchem-207 25 5 an an DET eurjchem-207 25 6     SPACE eurjchem-207 25 7 equimolar equimolar NOUN eurjchem-207 25 8     SPACE eurjchem-207 25 9 quantity quantity NOUN eurjchem-207 25 10     SPACE eurjchem-207 25 11 of of ADP eurjchem-207 25 12     SPACE eurjchem-207 25 13 ethyl ethyl PROPN eurjchem-207 25 14     SPACE eurjchem-207 26 1 4‐aminobenzoate 4‐aminobenzoate PROPN eurjchem-207 26 2     SPACE eurjchem-207 26 3 with with ADP eurjchem-207 26 4     SPACE eurjchem-207 26 5 3‐chlorobenzoyl 3‐chlorobenzoyl PROPN eurjchem-207 26 6     SPACE eurjchem-207 26 7 chloride chloride NOUN eurjchem-207 26 8     SPACE eurjchem-207 26 9 in in ADP eurjchem-207 26 10     SPACE eurjchem-207 26 11 dry dry ADJ eurjchem-207 26 12     SPACE eurjchem-207 26 13 thf thf NOUN eurjchem-207 26 14     SPACE eurjchem-207 26 15 afforded afford VERB eurjchem-207 26 16     SPACE eurjchem-207 26 17 the the DET eurjchem-207 26 18     SPACE eurjchem-207 26 19 title title NOUN eurjchem-207 26 20     SPACE eurjchem-207 26 21 amide amide NOUN eurjchem-207 26 22     SPACE eurjchem-207 26 23 ( ( PUNCT eurjchem-207 26 24 i i NOUN eurjchem-207 26 25 ) ) PUNCT eurjchem-207 26 26     SPACE eurjchem-207 26 27 in in ADP eurjchem-207 26 28     SPACE eurjchem-207 26 29 81 81 NUM eurjchem-207 26 30 % % NOUN eurjchem-207 26 31     SPACE eurjchem-207 26 32 yield yield NOUN eurjchem-207 26 33     SPACE eurjchem-207 26 34 ( ( PUNCT eurjchem-207 26 35 scheme scheme NOUN eurjchem-207 26 36     SPACE eurjchem-207 26 37 1 1 NUM eurjchem-207 26 38 ) ) PUNCT eurjchem-207 26 39 . . PUNCT eurjchem-207 26 40     SPACE eurjchem-207 27 1 the the DET eurjchem-207 27 2     SPACE eurjchem-207 27 3 ester ester NOUN eurjchem-207 27 4     SPACE eurjchem-207 27 5 amide amide NOUN eurjchem-207 27 6     SPACE eurjchem-207 27 7 was be AUX eurjchem-207 27 8     SPACE eurjchem-207 27 9 characterized characterize VERB eurjchem-207 27 10     SPACE eurjchem-207 27 11 by by ADP eurjchem-207 27 12     SPACE eurjchem-207 27 13 typical typical ADJ eurjchem-207 27 14     SPACE eurjchem-207 27 15 ir ir VERB eurjchem-207 27 16     SPACE eurjchem-207 27 17 stretching stretch VERB eurjchem-207 27 18     SPACE eurjchem-207 27 19 vibrations vibration NOUN eurjchem-207 27 20     SPACE eurjchem-207 27 21 for for ADP eurjchem-207 27 22     SPACE eurjchem-207 27 23 νnh νnh NOUN eurjchem-207 27 24     SPACE eurjchem-207 27 25 ( ( PUNCT eurjchem-207 27 26 3300 3300 NUM eurjchem-207 27 27 ) ) PUNCT eurjchem-207 27 28 , , PUNCT eurjchem-207 27 29     SPACE eurjchem-207 27 30 νc νc X eurjchem-207 27 31 = = NOUN eurjchem-207 27 32 o o NOUN eurjchem-207 27 33     SPACE eurjchem-207 27 34 ( ( PUNCT eurjchem-207 27 35 1665 1665 NUM eurjchem-207 27 36 ) ) PUNCT eurjchem-207 27 37 , , PUNCT eurjchem-207 27 38     SPACE eurjchem-207 27 39 νc‐o νc‐o PROPN eurjchem-207 27 40     SPACE eurjchem-207 27 41 ( ( PUNCT eurjchem-207 27 42 1290 1290 NUM eurjchem-207 27 43 ) ) PUNCT eurjchem-207 27 44 , , PUNCT eurjchem-207 27 45     SPACE eurjchem-207 27 46 νc−n νc−n PROPN eurjchem-207 27 47     SPACE eurjchem-207 27 48 ( ( PUNCT eurjchem-207 27 49 1154 1154 NUM eurjchem-207 27 50 ) ) PUNCT eurjchem-207 27 51     SPACE eurjchem-207 27 52 and and CCONJ eurjchem-207 27 53     SPACE eurjchem-207 27 54 ester ester NOUN eurjchem-207 27 55     SPACE eurjchem-207 27 56 νc νc NOUN eurjchem-207 27 57 = = NOUN eurjchem-207 27 58 o o NOUN eurjchem-207 27 59     SPACE eurjchem-207 27 60 ( ( PUNCT eurjchem-207 27 61 1721 1721 NUM eurjchem-207 27 62 ) ) PUNCT eurjchem-207 27 63     SPACE eurjchem-207 27 64 and and CCONJ eurjchem-207 27 65     SPACE eurjchem-207 27 66 1593 1593 NUM eurjchem-207 27 67     SPACE eurjchem-207 27 68 ( ( PUNCT eurjchem-207 27 69 aromatic aromatic NOUN eurjchem-207 27 70     SPACE eurjchem-207 27 71 ring ring NOUN eurjchem-207 27 72 ) ) PUNCT eurjchem-207 27 73     SPACE eurjchem-207 27 74 cm−1 cm−1 NOUN eurjchem-207 27 75 , , PUNCT eurjchem-207 27 76     SPACE eurjchem-207 27 77 respectively respectively ADV eurjchem-207 27 78 . . PUNCT eurjchem-207 27 79     SPACE eurjchem-207 27 80 in in ADP eurjchem-207 27 81     SPACE eurjchem-207 27 82 1h 1h NUM eurjchem-207 27 83     SPACE eurjchem-207 27 84 nmr nmr NOUN eurjchem-207 27 85     SPACE eurjchem-207 27 86 the the DET eurjchem-207 27 87     SPACE eurjchem-207 27 88 characteristic characteristic ADJ eurjchem-207 27 89     SPACE eurjchem-207 27 90 broad broad ADJ eurjchem-207 27 91     SPACE eurjchem-207 27 92 singlet singlet NOUN eurjchem-207 27 93     SPACE eurjchem-207 27 94 for for ADP eurjchem-207 27 95     SPACE eurjchem-207 27 96 the the DET eurjchem-207 27 97     SPACE eurjchem-207 27 98 amide amide NOUN eurjchem-207 27 99     SPACE eurjchem-207 27 100 proton proton NOUN eurjchem-207 27 101     SPACE eurjchem-207 27 102 appeared appear VERB eurjchem-207 27 103     SPACE eurjchem-207 27 104 at at ADP eurjchem-207 27 105     SPACE eurjchem-207 27 106   NUM eurjchem-207 27 107     SPACE eurjchem-207 27 108 9.09 9.09 NUM eurjchem-207 27 109     SPACE eurjchem-207 27 110 ppm ppm NOUN eurjchem-207 27 111     SPACE eurjchem-207 27 112 besides besides SCONJ eurjchem-207 27 113     SPACE eurjchem-207 27 114 the the DET eurjchem-207 27 115     SPACE eurjchem-207 27 116 signals signal NOUN eurjchem-207 27 117     SPACE eurjchem-207 27 118 for for ADP eurjchem-207 27 119     SPACE eurjchem-207 27 120 aromatic aromatic ADJ eurjchem-207 27 121     SPACE eurjchem-207 27 122 protons proton NOUN eurjchem-207 27 123     SPACE eurjchem-207 27 124 at at ADP eurjchem-207 27 125     SPACE eurjchem-207 27 126   NUM eurjchem-207 27 127     SPACE eurjchem-207 27 128 6.62‐7.16 6.62‐7.16 NUM eurjchem-207 27 129     SPACE eurjchem-207 27 130 ppm ppm NOUN eurjchem-207 27 131     SPACE eurjchem-207 27 132 and and CCONJ eurjchem-207 27 133     SPACE eurjchem-207 27 134 the the DET eurjchem-207 27 135     SPACE eurjchem-207 27 136 triplet triplet NOUN eurjchem-207 27 137     SPACE eurjchem-207 27 138 and and CCONJ eurjchem-207 27 139     SPACE eurjchem-207 27 140 quartet quartet NOUN eurjchem-207 27 141     SPACE eurjchem-207 27 142 for for ADP eurjchem-207 27 143     SPACE eurjchem-207 27 144 the the DET eurjchem-207 27 145     SPACE eurjchem-207 27 146 ethyl ethyl PROPN eurjchem-207 27 147     SPACE eurjchem-207 27 148 moiety moiety NOUN eurjchem-207 27 149     SPACE eurjchem-207 27 150 at at ADP eurjchem-207 27 151     SPACE eurjchem-207 27 152   NUM eurjchem-207 27 153     SPACE eurjchem-207 27 154 1.94 1.94 NUM eurjchem-207 27 155     SPACE eurjchem-207 27 156 and and CCONJ eurjchem-207 27 157     SPACE eurjchem-207 27 158 3.44 3.44 NUM eurjchem-207 27 159     SPACE eurjchem-207 27 160 ppm ppm NOUN eurjchem-207 27 161 , , PUNCT eurjchem-207 27 162     SPACE eurjchem-207 27 163 respectively respectively ADV eurjchem-207 27 164 . . PUNCT eurjchem-207 27 165     SPACE eurjchem-207 28 1 the the DET eurjchem-207 28 2     SPACE eurjchem-207 28 3 mass mass ADJ eurjchem-207 28 4     SPACE eurjchem-207 28 5 spectrum spectrum NOUN eurjchem-207 28 6     SPACE eurjchem-207 28 7 of of ADP eurjchem-207 28 8     SPACE eurjchem-207 28 9 the the DET eurjchem-207 28 10     SPACE eurjchem-207 28 11 compound compound NOUN eurjchem-207 28 12     SPACE eurjchem-207 28 13 showed show VERB eurjchem-207 28 14     SPACE eurjchem-207 28 15 the the DET eurjchem-207 28 16     SPACE eurjchem-207 28 17 molecular molecular ADJ eurjchem-207 28 18     SPACE eurjchem-207 28 19 ion ion NOUN eurjchem-207 28 20     SPACE eurjchem-207 28 21 peaks peak NOUN eurjchem-207 28 22     SPACE eurjchem-207 28 23 at at ADP eurjchem-207 28 24     SPACE eurjchem-207 28 25 m m PROPN eurjchem-207 28 26 / / PROPN eurjchem-207 28 27 z z NOUN eurjchem-207 28 28     SPACE eurjchem-207 28 29 304 304 NUM eurjchem-207 28 30     SPACE eurjchem-207 28 31 and and CCONJ eurjchem-207 28 32     SPACE eurjchem-207 28 33 305 305 NUM eurjchem-207 28 34     SPACE eurjchem-207 28 35 and and CCONJ eurjchem-207 28 36     SPACE eurjchem-207 28 37 the the DET eurjchem-207 28 38     SPACE eurjchem-207 28 39 base base NOUN eurjchem-207 28 40     SPACE eurjchem-207 28 41 peak peak NOUN eurjchem-207 28 42     SPACE eurjchem-207 28 43 at at ADP eurjchem-207 28 44     SPACE eurjchem-207 28 45 m m PROPN eurjchem-207 28 46 / / PROPN eurjchem-207 28 47 z z NOUN eurjchem-207 28 48     SPACE eurjchem-207 28 49 138.9 138.9 NUM eurjchem-207 28 50 , , PUNCT eurjchem-207 28 51     SPACE eurjchem-207 28 52 which which PRON eurjchem-207 28 53     SPACE eurjchem-207 28 54 originated originate VERB eurjchem-207 28 55     SPACE eurjchem-207 28 56 from from ADP eurjchem-207 28 57     SPACE eurjchem-207 28 58 the the DET eurjchem-207 28 59     SPACE eurjchem-207 28 60 3‐chlorobenzoyl 3‐chlorobenzoyl PROPN eurjchem-207 28 61     SPACE eurjchem-207 28 62 cation cation NOUN eurjchem-207 28 63 . . PUNCT eurjchem-207 28 64             SPACE eurjchem-207 29 1 o o X eurjchem-207 30 1 o o X eurjchem-207 30 2 o o NOUN eurjchem-207 30 3 n n CCONJ eurjchem-207 30 4 h h NOUN eurjchem-207 30 5 cl cl NOUN eurjchem-207 30 6 cooh cooh NOUN eurjchem-207 30 7 h2n h2n PROPN eurjchem-207 30 8 co2c2h5 co2c2h5 PROPN eurjchem-207 30 9 h2n h2n PROPN eurjchem-207 30 10 cocl cocl NOUN eurjchem-207 30 11 cl cl NOUN eurjchem-207 30 12 c2h5oh c2h5oh PROPN eurjchem-207 30 13 / / SYM eurjchem-207 30 14 h2so4 h2so4 PROPN eurjchem-207 30 15 reflux reflux NOUN eurjchem-207 30 16 dry dry ADJ eurjchem-207 30 17 thf thf NOUN eurjchem-207 30 18 reflux reflux NOUN eurjchem-207 30 19 ( ( PUNCT eurjchem-207 30 20 i i NOUN eurjchem-207 30 21 ) ) PUNCT eurjchem-207 30 22 scheme scheme NOUN eurjchem-207 30 23     SPACE eurjchem-207 30 24 1 1 NUM eurjchem-207 30 25         SPACE eurjchem-207 30 26 the the DET eurjchem-207 30 27     SPACE eurjchem-207 30 28 molecular molecular ADJ eurjchem-207 30 29     SPACE eurjchem-207 30 30 structure structure NOUN eurjchem-207 30 31     SPACE eurjchem-207 30 32 of of ADP eurjchem-207 30 33     SPACE eurjchem-207 30 34 the the DET eurjchem-207 30 35     SPACE eurjchem-207 30 36 title title NOUN eurjchem-207 30 37     SPACE eurjchem-207 30 38 compound compound NOUN eurjchem-207 30 39     SPACE eurjchem-207 30 40 is be AUX eurjchem-207 30 41     SPACE eurjchem-207 30 42 depicted depict VERB eurjchem-207 30 43     SPACE eurjchem-207 30 44 in in ADP eurjchem-207 30 45     SPACE eurjchem-207 30 46 figure figure NOUN eurjchem-207 30 47     SPACE eurjchem-207 30 48 1 1 NUM eurjchem-207 30 49 . . PUNCT eurjchem-207 30 50     SPACE eurjchem-207 30 51 table table NOUN eurjchem-207 30 52     SPACE eurjchem-207 30 53 1 1 NUM eurjchem-207 30 54     SPACE eurjchem-207 30 55 gives give VERB eurjchem-207 30 56     SPACE eurjchem-207 30 57 the the DET eurjchem-207 30 58     SPACE eurjchem-207 30 59 crystal crystal NOUN eurjchem-207 30 60     SPACE eurjchem-207 30 61 data datum NOUN eurjchem-207 30 62     SPACE eurjchem-207 30 63 and and CCONJ eurjchem-207 30 64     SPACE eurjchem-207 30 65 structure structure NOUN eurjchem-207 30 66     SPACE eurjchem-207 30 67 refinement refinement NOUN eurjchem-207 30 68 . . PUNCT eurjchem-207 30 69     SPACE eurjchem-207 31 1 the the DET eurjchem-207 31 2     SPACE eurjchem-207 31 3 selected select VERB eurjchem-207 31 4     SPACE eurjchem-207 31 5 bond bond NOUN eurjchem-207 31 6     SPACE eurjchem-207 31 7 lengths length NOUN eurjchem-207 31 8     SPACE eurjchem-207 31 9 and and CCONJ eurjchem-207 31 10     SPACE eurjchem-207 31 11 angles angle NOUN eurjchem-207 31 12     SPACE eurjchem-207 31 13 as as ADV eurjchem-207 31 14     SPACE eurjchem-207 31 15 well well ADV eurjchem-207 31 16     SPACE eurjchem-207 31 17 as as SCONJ eurjchem-207 31 18     SPACE eurjchem-207 31 19 hydrogen hydrogen NOUN eurjchem-207 31 20     SPACE eurjchem-207 31 21 bond bond NOUN eurjchem-207 31 22     SPACE eurjchem-207 31 23 parameters parameter NOUN eurjchem-207 31 24     SPACE eurjchem-207 31 25 are be AUX eurjchem-207 31 26     SPACE eurjchem-207 31 27 presented present VERB eurjchem-207 31 28     SPACE eurjchem-207 31 29 in in ADP eurjchem-207 31 30     SPACE eurjchem-207 31 31 table table NOUN eurjchem-207 31 32     SPACE eurjchem-207 31 33 2 2 NUM eurjchem-207 31 34 . . PUNCT eurjchem-207 31 35     SPACE eurjchem-207 31 36 the the DET eurjchem-207 31 37     SPACE eurjchem-207 31 38 two two NUM eurjchem-207 31 39     SPACE eurjchem-207 31 40 aromatic aromatic ADJ eurjchem-207 31 41     SPACE eurjchem-207 31 42 rings ring NOUN eurjchem-207 31 43     SPACE eurjchem-207 31 44 are be AUX eurjchem-207 31 45     SPACE eurjchem-207 31 46 almost almost ADV eurjchem-207 31 47     SPACE eurjchem-207 31 48 coplanar coplanar ADJ eurjchem-207 31 49 ; ; PUNCT eurjchem-207 31 50     SPACE eurjchem-207 31 51 the the DET eurjchem-207 31 52     SPACE eurjchem-207 31 53 accompanying accompanying ADJ eurjchem-207 31 54     SPACE eurjchem-207 31 55 dihedral dihedral ADJ eurjchem-207 31 56     SPACE eurjchem-207 31 57 angle angle NOUN eurjchem-207 31 58     SPACE eurjchem-207 31 59 is be AUX eurjchem-207 31 60     SPACE eurjchem-207 31 61 8.4(1 8.4(1 NUM eurjchem-207 31 62 ) ) PUNCT eurjchem-207 31 63     SPACE eurjchem-207 31 64 ° ° PROPN eurjchem-207 31 65 . . PUNCT eurjchem-207 31 66     SPACE eurjchem-207 31 67 the the DET eurjchem-207 31 68     SPACE eurjchem-207 31 69 carboxylate carboxylate NOUN eurjchem-207 31 70     SPACE eurjchem-207 31 71 group group NOUN eurjchem-207 31 72     SPACE eurjchem-207 31 73 is be AUX eurjchem-207 31 74     SPACE eurjchem-207 31 75 also also ADV eurjchem-207 31 76     SPACE eurjchem-207 31 77 coplanar coplanar VERB eurjchem-207 31 78     SPACE eurjchem-207 31 79 to to ADP eurjchem-207 31 80     SPACE eurjchem-207 31 81 the the DET eurjchem-207 31 82     SPACE eurjchem-207 31 83 attached attach VERB eurjchem-207 31 84     SPACE eurjchem-207 31 85 phenyl phenyl NOUN eurjchem-207 31 86     SPACE eurjchem-207 31 87 ring ring NOUN eurjchem-207 31 88     SPACE eurjchem-207 31 89 with with ADP eurjchem-207 31 90     SPACE eurjchem-207 31 91 a a DET eurjchem-207 31 92     SPACE eurjchem-207 31 93 torsion torsion NOUN eurjchem-207 31 94     SPACE eurjchem-207 31 95 angle angle NOUN eurjchem-207 31 96     SPACE eurjchem-207 31 97 c10‐c11‐c14‐o2 c10‐c11‐c14‐o2 NOUN eurjchem-207 31 98     SPACE eurjchem-207 31 99 of of ADP eurjchem-207 31 100     SPACE eurjchem-207 31 101 – – PUNCT eurjchem-207 31 102 176.7(2 176.7(2 NUM eurjchem-207 31 103 ) ) PUNCT eurjchem-207 31 104     SPACE eurjchem-207 31 105 ° ° PROPN eurjchem-207 31 106 . . PUNCT eurjchem-207 31 107     SPACE eurjchem-207 31 108 the the DET eurjchem-207 31 109     SPACE eurjchem-207 31 110 crystal crystal NOUN eurjchem-207 31 111     SPACE eurjchem-207 31 112 packing packing NOUN eurjchem-207 31 113     SPACE eurjchem-207 31 114 exhibits exhibit VERB eurjchem-207 31 115     SPACE eurjchem-207 31 116 a a DET eurjchem-207 31 117     SPACE eurjchem-207 31 118 strong strong ADJ eurjchem-207 31 119     SPACE eurjchem-207 31 120 n‐h n‐h NOUN eurjchem-207 31 121 … … SYM eurjchem-207 31 122 o o NOUN eurjchem-207 31 123     SPACE eurjchem-207 31 124 ( ( PUNCT eurjchem-207 31 125 x‐1 x‐1 PROPN eurjchem-207 31 126 , , PUNCT eurjchem-207 31 127     SPACE eurjchem-207 31 128 y y PROPN eurjchem-207 31 129 , , PUNCT eurjchem-207 31 130     SPACE eurjchem-207 31 131 z z NOUN eurjchem-207 31 132 ) ) PUNCT eurjchem-207 31 133     SPACE eurjchem-207 31 134 interaction interaction NOUN eurjchem-207 31 135     SPACE eurjchem-207 31 136 that that PRON eurjchem-207 31 137     SPACE eurjchem-207 31 138 connects connect VERB eurjchem-207 31 139     SPACE eurjchem-207 31 140 molecules molecule NOUN eurjchem-207 31 141     SPACE eurjchem-207 31 142 to to ADP eurjchem-207 31 143     SPACE eurjchem-207 31 144 endless endless ADJ eurjchem-207 31 145     SPACE eurjchem-207 31 146 sheets sheet NOUN eurjchem-207 31 147     SPACE eurjchem-207 31 148 exten‐ exten‐ NOUN eurjchem-207 31 149 ded de VERB eurjchem-207 31 150     SPACE eurjchem-207 31 151 along along ADP eurjchem-207 31 152     SPACE eurjchem-207 31 153 the the DET eurjchem-207 31 154     SPACE eurjchem-207 31 155 [ [ X eurjchem-207 31 156 100 100 NUM eurjchem-207 31 157 ] ] PUNCT eurjchem-207 31 158     SPACE eurjchem-207 31 159 plane plane NOUN eurjchem-207 31 160 . . PUNCT eurjchem-207 31 161     SPACE eurjchem-207 32 1 the the DET eurjchem-207 32 2     SPACE eurjchem-207 32 3 planes plane NOUN eurjchem-207 32 4     SPACE eurjchem-207 32 5 of of ADP eurjchem-207 32 6     SPACE eurjchem-207 32 7 these these DET eurjchem-207 32 8     SPACE eurjchem-207 32 9 sheets sheet NOUN eurjchem-207 32 10     SPACE eurjchem-207 32 11 are be AUX eurjchem-207 32 12     SPACE eurjchem-207 32 13 then then ADV eurjchem-207 32 14     SPACE eurjchem-207 32 15 stacked stack VERB eurjchem-207 32 16     SPACE eurjchem-207 32 17 in in ADP eurjchem-207 32 18     SPACE eurjchem-207 32 19 the the DET eurjchem-207 32 20     SPACE eurjchem-207 32 21 [ [ X eurjchem-207 32 22 010 010 NUM eurjchem-207 32 23 ] ] SYM eurjchem-207 32 24     SPACE eurjchem-207 32 25 direction direction NOUN eurjchem-207 32 26     SPACE eurjchem-207 32 27 ( ( PUNCT eurjchem-207 32 28 figure figure NOUN eurjchem-207 32 29     SPACE eurjchem-207 32 30 2 2 NUM eurjchem-207 32 31 ) ) PUNCT eurjchem-207 32 32 . . PUNCT eurjchem-207 32 33                         SPACE eurjchem-207 33 1 figure figure NOUN eurjchem-207 33 2     SPACE eurjchem-207 33 3 2 2 NUM eurjchem-207 33 4 . . PUNCT eurjchem-207 33 5     SPACE eurjchem-207 33 6 crystal crystal NOUN eurjchem-207 33 7     SPACE eurjchem-207 33 8 packing packing NOUN eurjchem-207 33 9     SPACE eurjchem-207 33 10 viewed view VERB eurjchem-207 33 11     SPACE eurjchem-207 33 12 along along ADP eurjchem-207 33 13     SPACE eurjchem-207 34 1 [ [ X eurjchem-207 34 2 100 100 NUM eurjchem-207 34 3 ] ] PUNCT eurjchem-207 34 4     SPACE eurjchem-207 34 5 with with ADP eurjchem-207 34 6     SPACE eurjchem-207 34 7 hydrogen hydrogen NOUN eurjchem-207 34 8     SPACE eurjchem-207 34 9 bonds bond NOUN eurjchem-207 34 10     SPACE eurjchem-207 34 11 as as ADP eurjchem-207 34 12     SPACE eurjchem-207 34 13 dotted dotted ADJ eurjchem-207 34 14     SPACE eurjchem-207 34 15 lines line NOUN eurjchem-207 34 16 . . PUNCT eurjchem-207 34 17     SPACE eurjchem-207 34 18 hydrogen hydrogen NOUN eurjchem-207 34 19     SPACE eurjchem-207 34 20 atoms atom NOUN eurjchem-207 34 21     SPACE eurjchem-207 34 22 not not PART eurjchem-207 34 23     SPACE eurjchem-207 34 24 involved involve VERB eurjchem-207 34 25     SPACE eurjchem-207 34 26 in in ADP eurjchem-207 34 27     SPACE eurjchem-207 34 28 bonding bonding NOUN eurjchem-207 34 29     SPACE eurjchem-207 34 30 pattern pattern NOUN eurjchem-207 34 31     SPACE eurjchem-207 34 32 are be AUX eurjchem-207 34 33     SPACE eurjchem-207 34 34 omitted omit VERB eurjchem-207 34 35 . . PUNCT eurjchem-207 34 36         SPACE eurjchem-207 35 1 table table NOUN eurjchem-207 35 2     SPACE eurjchem-207 35 3 2 2 NUM eurjchem-207 35 4 . . PUNCT eurjchem-207 35 5     SPACE eurjchem-207 35 6 selected select VERB eurjchem-207 35 7     SPACE eurjchem-207 35 8 geometric geometric ADJ eurjchem-207 35 9     SPACE eurjchem-207 35 10 parameters parameter NOUN eurjchem-207 35 11     SPACE eurjchem-207 35 12 ( ( PUNCT eurjchem-207 35 13 å å PROPN eurjchem-207 35 14 , , PUNCT eurjchem-207 35 15     SPACE eurjchem-207 35 16 ° ° NOUN eurjchem-207 35 17 ) ) PUNCT eurjchem-207 35 18     SPACE eurjchem-207 35 19 for for ADP eurjchem-207 35 20     SPACE eurjchem-207 35 21 the the DET eurjchem-207 35 22     SPACE eurjchem-207 35 23 title title NOUN eurjchem-207 35 24     SPACE eurjchem-207 35 25 compound compound NOUN eurjchem-207 35 26 . . PUNCT eurjchem-207 35 27     SPACE eurjchem-207 36 1 bond bond NOUN eurjchem-207 36 2     SPACE eurjchem-207 36 3 distances distance NOUN eurjchem-207 36 4 cl1‐c2 cl1‐c2 PROPN eurjchem-207 36 5 1.742(2 1.742(2 NUM eurjchem-207 36 6 ) ) PUNCT eurjchem-207 36 7     SPACE eurjchem-207 36 8 o1‐c7 o1‐c7 VERB eurjchem-207 36 9 1.232(3 1.232(3 NUM eurjchem-207 36 10 ) ) PUNCT eurjchem-207 36 11     SPACE eurjchem-207 36 12 n1‐c7 n1‐c7 NOUN eurjchem-207 36 13 1.356(3 1.356(3 NUM eurjchem-207 36 14 ) ) PUNCT eurjchem-207 36 15     SPACE eurjchem-207 36 16 n1‐c8 n1‐c8 NOUN eurjchem-207 36 17 1.410(3 1.410(3 NUM eurjchem-207 36 18 ) ) PUNCT eurjchem-207 36 19     SPACE eurjchem-207 36 20 c6‐c7 c6‐c7 X eurjchem-207 36 21 1.486(3 1.486(3 NUM eurjchem-207 36 22 ) ) PUNCT eurjchem-207 36 23     SPACE eurjchem-207 36 24 n1‐h1b n1‐h1b NOUN eurjchem-207 36 25 0.88 0.88 NUM eurjchem-207 36 26     SPACE eurjchem-207 36 27 h1b h1b NOUN eurjchem-207 36 28 … … SYM eurjchem-207 36 29 o1i o1i ADJ eurjchem-207 36 30 2.29 2.29 NUM eurjchem-207 36 31     SPACE eurjchem-207 36 32 n1 n1 NOUN eurjchem-207 36 33 … … SYM eurjchem-207 36 34 o1 o1 NOUN eurjchem-207 36 35     SPACE eurjchem-207 36 36 i i PROPN eurjchem-207 36 37 3.110(2 3.110(2 NUM eurjchem-207 36 38 ) ) PUNCT eurjchem-207 36 39     SPACE eurjchem-207 36 40 bond bond NOUN eurjchem-207 36 41     SPACE eurjchem-207 36 42 angles angle VERB eurjchem-207 36 43 c7‐n1‐c8 c7‐n1‐c8 NOUN eurjchem-207 36 44 127.03(18 127.03(18 NUM eurjchem-207 36 45 ) ) PUNCT eurjchem-207 36 46     SPACE eurjchem-207 36 47 o1‐c7‐n1 o1‐c7‐n1 PROPN eurjchem-207 36 48 123.0(2 123.0(2 NUM eurjchem-207 36 49 ) ) PUNCT eurjchem-207 36 50     SPACE eurjchem-207 36 51 o1‐c7‐c6 o1‐c7‐c6 PROPN eurjchem-207 36 52 121.23(19 121.23(19 NUM eurjchem-207 36 53 ) ) PUNCT eurjchem-207 36 54     SPACE eurjchem-207 36 55 n1‐c7‐c6 n1‐c7‐c6 NOUN eurjchem-207 36 56     SPACE eurjchem-207 36 57 115.80(18 115.80(18 NUM eurjchem-207 36 58 ) ) PUNCT eurjchem-207 36 59     SPACE eurjchem-207 36 60 n1‐h1b n1‐h1b NOUN eurjchem-207 36 61 … … SYM eurjchem-207 36 62 o1 o1 NOUN eurjchem-207 36 63 155.2 155.2 NUM eurjchem-207 36 64     SPACE eurjchem-207 36 65 symmetry symmetry NOUN eurjchem-207 36 66     SPACE eurjchem-207 36 67 code code NOUN eurjchem-207 36 68 : : PUNCT eurjchem-207 36 69     SPACE eurjchem-207 36 70 ( ( PUNCT eurjchem-207 36 71 i i NOUN eurjchem-207 36 72 ) ) PUNCT eurjchem-207 36 73     SPACE eurjchem-207 36 74 x‐1 x‐1 PROPN eurjchem-207 36 75 , , PUNCT eurjchem-207 36 76     SPACE eurjchem-207 36 77 y y PROPN eurjchem-207 36 78 , , PUNCT eurjchem-207 36 79     SPACE eurjchem-207 36 80 z. z. PROPN eurjchem-207 36 81         SPACE eurjchem-207 36 82 supplementary supplementary ADJ eurjchem-207 36 83     SPACE eurjchem-207 36 84 materials material NOUN eurjchem-207 36 85         SPACE eurjchem-207 36 86 ccdc‐679109 ccdc‐679109 VERB eurjchem-207 36 87     SPACE eurjchem-207 36 88 contains contain VERB eurjchem-207 36 89     SPACE eurjchem-207 36 90 the the DET eurjchem-207 36 91     SPACE eurjchem-207 36 92 supplementary supplementary ADJ eurjchem-207 36 93     SPACE eurjchem-207 36 94 crystallographic crystallographic ADJ eurjchem-207 36 95     SPACE eurjchem-207 36 96 data datum NOUN eurjchem-207 36 97     SPACE eurjchem-207 36 98 for for ADP eurjchem-207 36 99     SPACE eurjchem-207 36 100 this this DET eurjchem-207 36 101     SPACE eurjchem-207 36 102 paper paper NOUN eurjchem-207 36 103 . . PUNCT eurjchem-207 36 104     SPACE eurjchem-207 37 1 these these DET eurjchem-207 37 2     SPACE eurjchem-207 37 3 data datum NOUN eurjchem-207 37 4     SPACE eurjchem-207 37 5 can can AUX eurjchem-207 37 6     SPACE eurjchem-207 37 7 be be AUX eurjchem-207 37 8     SPACE eurjchem-207 37 9 obtained obtain VERB eurjchem-207 37 10     SPACE eurjchem-207 37 11 free free ADJ eurjchem-207 37 12     SPACE eurjchem-207 37 13 of of ADP eurjchem-207 37 14     SPACE eurjchem-207 37 15 charge charge NOUN eurjchem-207 37 16     SPACE eurjchem-207 37 17 via via ADP eurjchem-207 37 18     SPACE eurjchem-207 37 19 www.ccdc.cam.ac.uk/data_request/cif www.ccdc.cam.ac.uk/data_request/cif NOUN eurjchem-207 37 20 , , PUNCT eurjchem-207 37 21     SPACE eurjchem-207 37 22 or or CCONJ eurjchem-207 37 23     SPACE eurjchem-207 37 24 by by ADP eurjchem-207 37 25     SPACE eurjchem-207 37 26 e‐mailing e‐mailing NOUN eurjchem-207 37 27     SPACE eurjchem-207 37 28 data_request@ccdc.cam.ac.uk data_request@ccdc.cam.ac.uk PROPN eurjchem-207 37 29 , , PUNCT eurjchem-207 37 30     SPACE eurjchem-207 37 31 or or CCONJ eurjchem-207 37 32     SPACE eurjchem-207 37 33 by by ADP eurjchem-207 37 34     SPACE eurjchem-207 37 35 contacting contact VERB eurjchem-207 37 36     SPACE eurjchem-207 37 37 the the DET eurjchem-207 37 38     SPACE eurjchem-207 37 39 cambridge cambridge PROPN eurjchem-207 37 40     SPACE eurjchem-207 37 41 crystallographic crystallographic ADJ eurjchem-207 37 42     SPACE eurjchem-207 37 43 data data NOUN eurjchem-207 37 44     SPACE eurjchem-207 37 45 centre centre NOUN eurjchem-207 37 46 , , PUNCT eurjchem-207 37 47     SPACE eurjchem-207 37 48 12 12 NUM eurjchem-207 37 49     SPACE eurjchem-207 37 50 union union NOUN eurjchem-207 37 51     SPACE eurjchem-207 37 52 road road NOUN eurjchem-207 37 53 , , PUNCT eurjchem-207 37 54     SPACE eurjchem-207 37 55 cambridge cambridge PROPN eurjchem-207 37 56     SPACE eurjchem-207 37 57 cb2 cb2 PROPN eurjchem-207 37 58     SPACE eurjchem-207 37 59 1ez 1ez NOUN eurjchem-207 37 60 , , PUNCT eurjchem-207 37 61     SPACE eurjchem-207 37 62 uk uk PROPN eurjchem-207 37 63 ; ; PUNCT eurjchem-207 37 64     SPACE eurjchem-207 37 65 fax fax NOUN eurjchem-207 37 66 : : PUNCT eurjchem-207 37 67     SPACE eurjchem-207 37 68 +44(0)1223‐336033 +44(0)1223‐336033 ADJ eurjchem-207 37 69 . . PUNCT eurjchem-207 37 70         SPACE eurjchem-207 37 71 references reference NOUN eurjchem-207 37 72         SPACE eurjchem-207 38 1 [ [ X eurjchem-207 38 2 1 1 NUM eurjchem-207 38 3 ] ] PUNCT eurjchem-207 38 4 . . PUNCT eurjchem-207 39 1 omar omar PROPN eurjchem-207 39 2 , , PUNCT eurjchem-207 39 3     SPACE eurjchem-207 39 4 f. f. PROPN eurjchem-207 39 5     SPACE eurjchem-207 39 6 a. a. NOUN eurjchem-207 39 7 ; ; PUNCT eurjchem-207 39 8     SPACE eurjchem-207 39 9 mahfouz mahfouz ADJ eurjchem-207 39 10 , , PUNCT eurjchem-207 39 11     SPACE eurjchem-207 39 12 n. n. NOUN eurjchem-207 39 13     SPACE eurjchem-207 39 14 m. m. NOUN eurjchem-207 39 15 ; ; PUNCT eurjchem-207 39 16     SPACE eurjchem-207 39 17 rahman rahman PROPN eurjchem-207 39 18 , , PUNCT eurjchem-207 39 19     SPACE eurjchem-207 39 20 m. m. NOUN eurjchem-207 39 21     SPACE eurjchem-207 39 22 a. a. NOUN eurjchem-207 39 23     SPACE eurjchem-207 39 24 eur eur PROPN eurjchem-207 39 25 . . PUNCT eurjchem-207 39 26     SPACE eurjchem-207 39 27 j. j. PROPN eurjchem-207 39 28     SPACE eurjchem-207 39 29 med med PROPN eurjchem-207 39 30 . . PUNCT eurjchem-207 39 31     SPACE eurjchem-207 39 32 chem chem NOUN eurjchem-207 39 33 . . PUNCT eurjchem-207 39 34     SPACE eurjchem-207 39 35 1996 1996 NUM eurjchem-207 39 36 , , PUNCT eurjchem-207 39 37     SPACE eurjchem-207 39 38 31 31 NUM eurjchem-207 39 39 , , PUNCT eurjchem-207 39 40     SPACE eurjchem-207 39 41 819‐825 819‐825 NUM eurjchem-207 39 42 . . PUNCT eurjchem-207 39 43     SPACE eurjchem-207 40 1 [ [ X eurjchem-207 40 2 2 2 NUM eurjchem-207 40 3 ] ] PUNCT eurjchem-207 40 4 . . PUNCT eurjchem-207 41 1 amir amir PROPN eurjchem-207 41 2 , , PUNCT eurjchem-207 41 3     SPACE eurjchem-207 41 4 m. m. NOUN eurjchem-207 41 5 ; ; PUNCT eurjchem-207 41 6     SPACE eurjchem-207 41 7 oberoi oberoi NOUN eurjchem-207 41 8 , , PUNCT eurjchem-207 41 9     SPACE eurjchem-207 41 10 a. a. NOUN eurjchem-207 41 11 ; ; PUNCT eurjchem-207 41 12     SPACE eurjchem-207 41 13 alam alam PROPN eurjchem-207 41 14 , , PUNCT eurjchem-207 41 15     SPACE eurjchem-207 41 16 s. s. PROPN eurjchem-207 41 17     SPACE eurjchem-207 41 18 indian indian PROPN eurjchem-207 41 19     SPACE eurjchem-207 41 20 j. j. PROPN eurjchem-207 41 21     SPACE eurjchem-207 41 22 chem chem NOUN eurjchem-207 41 23 . . PUNCT eurjchem-207 41 24     SPACE eurjchem-207 41 25 1999 1999 NUM eurjchem-207 41 26 , , PUNCT eurjchem-207 41 27     SPACE eurjchem-207 41 28 38b 38b NOUN eurjchem-207 41 29 , , PUNCT eurjchem-207 41 30     SPACE eurjchem-207 41 31 237‐242 237‐242 PROPN eurjchem-207 41 32 . . PUNCT eurjchem-207 41 33     SPACE eurjchem-207 42 1 [ [ X eurjchem-207 42 2 3 3 NUM eurjchem-207 42 3 ] ] PUNCT eurjchem-207 42 4 . . PUNCT eurjchem-207 43 1 palaska palaska PROPN eurjchem-207 43 2 , , PUNCT eurjchem-207 43 3     SPACE eurjchem-207 43 4 e. e. PROPN eurjchem-207 43 5 ; ; PUNCT eurjchem-207 43 6     SPACE eurjchem-207 43 7 sahin sahin PROPN eurjchem-207 43 8 , , PUNCT eurjchem-207 43 9     SPACE eurjchem-207 43 10 g. g. NOUN eurjchem-207 43 11 ; ; PUNCT eurjchem-207 43 12     SPACE eurjchem-207 43 13 kelicen kelicen NOUN eurjchem-207 43 14 , , PUNCT eurjchem-207 43 15     SPACE eurjchem-207 43 16 p. p. NOUN eurjchem-207 43 17 ; ; PUNCT eurjchem-207 43 18     SPACE eurjchem-207 43 19 durlu durlu NOUN eurjchem-207 43 20 , , PUNCT eurjchem-207 43 21     SPACE eurjchem-207 43 22 n. n. NOUN eurjchem-207 43 23     SPACE eurjchem-207 43 24 t. t. PROPN eurjchem-207 43 25 ; ; PUNCT eurjchem-207 43 26     SPACE eurjchem-207 43 27 altinok altinok PROPN eurjchem-207 43 28 , , PUNCT eurjchem-207 43 29     SPACE eurjchem-207 43 30 g. g. NOUN eurjchem-207 43 31     SPACE eurjchem-207 43 32 farmaco farmaco PROPN eurjchem-207 43 33     SPACE eurjchem-207 43 34 2002 2002 NUM eurjchem-207 43 35 , , PUNCT eurjchem-207 43 36     SPACE eurjchem-207 43 37 57 57 NUM eurjchem-207 43 38 , , PUNCT eurjchem-207 43 39     SPACE eurjchem-207 43 40 101‐107 101‐107 PROPN eurjchem-207 43 41 . . PUNCT eurjchem-207 43 42     SPACE eurjchem-207 44 1 [ [ X eurjchem-207 44 2 4 4 NUM eurjchem-207 44 3 ] ] PUNCT eurjchem-207 44 4 . . PUNCT eurjchem-207 45 1 kumar kumar PROPN eurjchem-207 45 2 , , PUNCT eurjchem-207 45 3     SPACE eurjchem-207 45 4 a. a. NOUN eurjchem-207 45 5 ; ; PUNCT eurjchem-207 45 6     SPACE eurjchem-207 45 7 bansal bansal NOUN eurjchem-207 45 8 , , PUNCT eurjchem-207 45 9     SPACE eurjchem-207 45 10 d. d. PROPN eurjchem-207 45 11 ; ; PUNCT eurjchem-207 45 12     SPACE eurjchem-207 45 13 bajaj bajaj PROPN eurjchem-207 45 14 , , PUNCT eurjchem-207 45 15     SPACE eurjchem-207 45 16 k. k. PROPN eurjchem-207 45 17 ; ; PUNCT eurjchem-207 45 18     SPACE eurjchem-207 45 19 sharma sharma NOUN eurjchem-207 45 20 , , PUNCT eurjchem-207 45 21     SPACE eurjchem-207 45 22 s. s. PROPN eurjchem-207 45 23 ; ; PUNCT eurjchem-207 45 24     SPACE eurjchem-207 45 25 archana archana PROPN eurjchem-207 45 26 , , PUNCT eurjchem-207 45 27     SPACE eurjchem-207 45 28 k. k. PROPN eurjchem-207 45 29 ; ; PUNCT eurjchem-207 45 30     SPACE eurjchem-207 45 31 srivastava srivastava PROPN eurjchem-207 45 32 , , PUNCT eurjchem-207 45 33     SPACE eurjchem-207 45 34 v. v. ADP eurjchem-207 45 35     SPACE eurjchem-207 45 36 k. k. NOUN eurjchem-207 45 37     SPACE eurjchem-207 45 38 bioorg bioorg PROPN eurjchem-207 45 39 . . PUNCT eurjchem-207 45 40     SPACE eurjchem-207 45 41 med med PROPN eurjchem-207 45 42 . . PUNCT eurjchem-207 45 43     SPACE eurjchem-207 45 44 chem chem NOUN eurjchem-207 45 45 . . PUNCT eurjchem-207 45 46     SPACE eurjchem-207 45 47 2003 2003 NUM eurjchem-207 45 48 , , PUNCT eurjchem-207 45 49     SPACE eurjchem-207 45 50 11 11 NUM eurjchem-207 45 51 , , PUNCT eurjchem-207 45 52     SPACE eurjchem-207 45 53 5281‐5291 5281‐5291 NUM eurjchem-207 45 54 . . PUNCT eurjchem-207 45 55     SPACE eurjchem-207 46 1 [ [ X eurjchem-207 46 2 5 5 NUM eurjchem-207 46 3 ] ] PUNCT eurjchem-207 46 4 . . PUNCT eurjchem-207 47 1 jackson jackson PROPN eurjchem-207 47 2 , , PUNCT eurjchem-207 47 3     SPACE eurjchem-207 47 4 s. s. PROPN eurjchem-207 47 5 ; ; PUNCT eurjchem-207 47 6     SPACE eurjchem-207 47 7 degrado degrado PROPN eurjchem-207 47 8 , , PUNCT eurjchem-207 47 9     SPACE eurjchem-207 47 10 w. w. NOUN eurjchem-207 47 11 ; ; PUNCT eurjchem-207 47 12     SPACE eurjchem-207 47 13 dwivedi dwivedi NOUN eurjchem-207 47 14 , , PUNCT eurjchem-207 47 15     SPACE eurjchem-207 47 16 a. a. NOUN eurjchem-207 47 17 ; ; PUNCT eurjchem-207 47 18     SPACE eurjchem-207 47 19 parthasarathy parthasarathy ADJ eurjchem-207 47 20 , , PUNCT eurjchem-207 47 21     SPACE eurjchem-207 47 22 a. a. NOUN eurjchem-207 47 23 ; ; PUNCT eurjchem-207 47 24     SPACE eurjchem-207 47 25 higley higley PROPN eurjchem-207 47 26 , , PUNCT eurjchem-207 47 27     SPACE eurjchem-207 47 28 a. a. NOUN eurjchem-207 47 29 ; ; PUNCT eurjchem-207 47 30     SPACE eurjchem-207 47 31 krywko krywko NOUN eurjchem-207 47 32 , , PUNCT eurjchem-207 47 33     SPACE eurjchem-207 47 34 j. j. PROPN eurjchem-207 47 35 ; ; PUNCT eurjchem-207 47 36     SPACE eurjchem-207 47 37 rockwell rockwell VERB eurjchem-207 47 38 , , PUNCT eurjchem-207 47 39     SPACE eurjchem-207 47 40 a. a. NOUN eurjchem-207 47 41 ; ; PUNCT eurjchem-207 47 42     SPACE eurjchem-207 47 43 markwalder markwalder NOUN eurjchem-207 47 44 , , PUNCT eurjchem-207 47 45     SPACE eurjchem-207 47 46 j. j. PROPN eurjchem-207 47 47 ; ; PUNCT eurjchem-207 47 48     SPACE eurjchem-207 47 49 wells well NOUN eurjchem-207 47 50 , , PUNCT eurjchem-207 47 51     SPACE eurjchem-207 47 52 g. g. NOUN eurjchem-207 47 53 ; ; PUNCT eurjchem-207 47 54     SPACE eurjchem-207 47 55 wexler wexler NOUN eurjchem-207 47 56 , , PUNCT eurjchem-207 47 57     SPACE eurjchem-207 47 58 r. r. PROPN eurjchem-207 47 59 ; ; PUNCT eurjchem-207 47 60     SPACE eurjchem-207 47 61 mousa mousa NOUN eurjchem-207 47 62 , , PUNCT eurjchem-207 47 63     SPACE eurjchem-207 47 64 s. s. PROPN eurjchem-207 47 65 ; ; PUNCT eurjchem-207 47 66       SPACE eurjchem-207 47 67 harlow harlow NOUN eurjchem-207 47 68 , , PUNCT eurjchem-207 47 69     SPACE eurjchem-207 47 70 r. r. PROPN eurjchem-207 47 71     SPACE eurjchem-207 47 72 j. j. PROPN eurjchem-207 47 73     SPACE eurjchem-207 47 74 am be AUX eurjchem-207 47 75 . . PUNCT eurjchem-207 47 76     SPACE eurjchem-207 47 77 chem chem NOUN eurjchem-207 47 78 . . PUNCT eurjchem-207 47 79     SPACE eurjchem-207 47 80 soc soc PROPN eurjchem-207 47 81 . . PUNCT eurjchem-207 47 82     SPACE eurjchem-207 47 83 1994 1994 NUM eurjchem-207 47 84 , , PUNCT eurjchem-207 47 85     SPACE eurjchem-207 47 86 116 116 NUM eurjchem-207 47 87 , , PUNCT eurjchem-207 47 88     SPACE eurjchem-207 47 89 3220‐3230 3220‐3230 NUM eurjchem-207 47 90 . . PUNCT eurjchem-207 47 91     SPACE eurjchem-207 48 1 [ [ X eurjchem-207 48 2 6 6 NUM eurjchem-207 48 3 ] ] PUNCT eurjchem-207 48 4 . . PUNCT eurjchem-207 48 5 capdeville capdeville PROPN eurjchem-207 48 6 , , PUNCT eurjchem-207 48 7     SPACE eurjchem-207 48 8 r. r. PROPN eurjchem-207 48 9 ; ; PUNCT eurjchem-207 48 10     SPACE eurjchem-207 48 11 buchdunger buchdunger NOUN eurjchem-207 48 12 , , PUNCT eurjchem-207 48 13     SPACE eurjchem-207 48 14 e. e. PROPN eurjchem-207 48 15 ; ; PUNCT eurjchem-207 48 16     SPACE eurjchem-207 48 17 zimmermann zimmermann PROPN eurjchem-207 48 18 , , PUNCT eurjchem-207 48 19     SPACE eurjchem-207 48 20 j. j. PROPN eurjchem-207 48 21 ; ; PUNCT eurjchem-207 48 22     SPACE eurjchem-207 48 23 matter matter NOUN eurjchem-207 48 24 , , PUNCT eurjchem-207 48 25     SPACE eurjchem-207 48 26 j. j. PROPN eurjchem-207 48 27     SPACE eurjchem-207 48 28 nat nat PROPN eurjchem-207 48 29 . . PUNCT eurjchem-207 48 30     SPACE eurjchem-207 48 31 rev rev VERB eurjchem-207 48 32 . . PROPN eurjchem-207 48 33     SPACE eurjchem-207 48 34 drug drug NOUN eurjchem-207 48 35     SPACE eurjchem-207 48 36 discovery discovery NOUN eurjchem-207 48 37 . . PUNCT eurjchem-207 48 38     SPACE eurjchem-207 49 1 2002 2002 NUM eurjchem-207 49 2 , , PUNCT eurjchem-207 49 3     SPACE eurjchem-207 49 4 1 1 NUM eurjchem-207 49 5 , , PUNCT eurjchem-207 49 6     SPACE eurjchem-207 49 7 493‐502 493‐502 NOUN eurjchem-207 49 8 . . PUNCT eurjchem-207 49 9     SPACE eurjchem-207 50 1 [ [ X eurjchem-207 50 2 7 7 NUM eurjchem-207 50 3 ] ] PUNCT eurjchem-207 50 4 . . PUNCT eurjchem-207 50 5 manley manley PROPN eurjchem-207 50 6 , , PUNCT eurjchem-207 50 7     SPACE eurjchem-207 50 8 p. p. NOUN eurjchem-207 50 9     SPACE eurjchem-207 50 10 w. w. PROPN eurjchem-207 50 11 ; ; PUNCT eurjchem-207 50 12     SPACE eurjchem-207 50 13 furet furet PROPN eurjchem-207 50 14 , , PUNCT eurjchem-207 50 15     SPACE eurjchem-207 50 16 p. p. NOUN eurjchem-207 50 17 ; ; PUNCT eurjchem-207 50 18     SPACE eurjchem-207 50 19 bold bold ADJ eurjchem-207 50 20 , , PUNCT eurjchem-207 50 21     SPACE eurjchem-207 50 22 g. g. NOUN eurjchem-207 50 23 ; ; PUNCT eurjchem-207 50 24     SPACE eurjchem-207 50 25 bruggen bruggen NOUN eurjchem-207 50 26 , , PUNCT eurjchem-207 50 27     SPACE eurjchem-207 50 28 j. j. PROPN eurjchem-207 50 29 ; ; PUNCT eurjchem-207 50 30     SPACE eurjchem-207 50 31 mestan mestan ADJ eurjchem-207 50 32 , , PUNCT eurjchem-207 50 33     SPACE eurjchem-207 50 34 j. j. PROPN eurjchem-207 50 35 ; ; PUNCT eurjchem-207 50 36     SPACE eurjchem-207 50 37 meyer meyer PROPN eurjchem-207 50 38 , , PUNCT eurjchem-207 50 39     SPACE eurjchem-207 50 40 t. t. PROPN eurjchem-207 50 41 ; ; PUNCT eurjchem-207 50 42     SPACE eurjchem-207 50 43 schnell schnell PROPN eurjchem-207 50 44 , , PUNCT eurjchem-207 50 45     SPACE eurjchem-207 50 46 c. c. PROPN eurjchem-207 50 47     SPACE eurjchem-207 50 48 r. r. PROPN eurjchem-207 50 49 ; ; PUNCT eurjchem-207 50 50     SPACE eurjchem-207 50 51 wood wood NOUN eurjchem-207 50 52 , , PUNCT eurjchem-207 50 53     SPACE eurjchem-207 50 54 j. j. PROPN eurjchem-207 50 55     SPACE eurjchem-207 50 56 j. j. PROPN eurjchem-207 50 57     SPACE eurjchem-207 50 58 med med PROPN eurjchem-207 50 59 . . PUNCT eurjchem-207 50 60     SPACE eurjchem-207 50 61 chem chem NOUN eurjchem-207 50 62 . . PUNCT eurjchem-207 50 63     SPACE eurjchem-207 50 64 2002 2002 NUM eurjchem-207 50 65 , , PUNCT eurjchem-207 50 66     SPACE eurjchem-207 50 67 45 45 NUM eurjchem-207 50 68 , , PUNCT eurjchem-207 50 69     SPACE eurjchem-207 50 70 5687‐5693 5687‐5693 NUM eurjchem-207 50 71 . . PUNCT eurjchem-207 50 72         SPACE