id	sid	tid	token	lemma	pos
eurjchem-208	1	1	untitled	untitle	VERB
eurjchem-208	1	2	european	european	PROPN
eurjchem-208	1	3	journal	journal	PROPN
eurjchem-208	1	4	of	of	ADP
eurjchem-208	1	5	chemistry	chemistry	NOUN
eurjchem-208	1	6	2	2	NUM
eurjchem-208	1	7	(	(	PUNCT
eurjchem-208	1	8	1	1	NUM
eurjchem-208	1	9	)	)	PUNCT
eurjchem-208	1	10	(	(	PUNCT
eurjchem-208	1	11	2011	2011	NUM
eurjchem-208	1	12	)	)	PUNCT
eurjchem-208	1	13	25‐35	25‐35	NUM
eurjchem-208	1	14	european	european	PROPN
eurjchem-208	1	15	journal	journal	PROPN
eurjchem-208	1	16	of	of	ADP
eurjchem-208	1	17	chemistry	chemistry	NOUN
eurjchem-208	1	18	issn	issn	PROPN
eurjchem-208	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-208	1	20	(	(	PUNCT
eurjchem-208	1	21	print	print	NOUN
eurjchem-208	1	22	)	)	PUNCT
eurjchem-208	1	23	/	/	SYM
eurjchem-208	1	24	issn	issn	PROPN
eurjchem-208	1	25	2153‐2257	2153‐2257	NUM
eurjchem-208	1	26	(	(	PUNCT
eurjchem-208	1	27	online	online	ADJ
eurjchem-208	1	28	)	)	PUNCT
eurjchem-208	1	29			NOUN
eurjchem-208	1	30	2011	2011	NUM
eurjchem-208	1	31	eurjchem	eurjchem	PROPN
eurjchem-208	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-208	1	33	/	/	SYM
eurjchem-208	1	34	eurjchem.2.1.25‐35.208	eurjchem.2.1.25‐35.208	NOUN
eurjchem-208	1	35	european	european	ADJ
eurjchem-208	1	36	journal	journal	NOUN
eurjchem-208	1	37	of	of	ADP
eurjchem-208	1	38	chemistry	chemistry	PROPN
eurjchem-208	1	39	journal	journal	PROPN
eurjchem-208	1	40	homepage	homepage	NOUN
eurjchem-208	1	41	:	:	PUNCT
eurjchem-208	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-208	1	43	synthesis	synthesis	NOUN
eurjchem-208	1	44	and	and	CCONJ
eurjchem-208	1	45	antimicrobial	antimicrobial	ADJ
eurjchem-208	1	46	activities	activity	NOUN
eurjchem-208	1	47	of	of	ADP
eurjchem-208	1	48	some	some	DET
eurjchem-208	1	49	novel	novel	ADJ
eurjchem-208	1	50	bis‐pyrazole	bis‐pyrazole	NOUN
eurjchem-208	1	51	derivatives	derivative	NOUN
eurjchem-208	1	52	containing	contain	VERB
eurjchem-208	1	53	a	a	DET
eurjchem-208	1	54	hydrophosphoryl	hydrophosphoryl	ADJ
eurjchem-208	1	55	unit	unit	NOUN
eurjchem-208	1	56	salah	salah	PROPN
eurjchem-208	1	57	abdel‐ghaffar	abdel‐ghaffar	ADV
eurjchem-208	1	58	abdel‐aziz	abdel‐aziz	PROPN
eurjchem-208	1	59	,	,	PUNCT
eurjchem-208	1	60	tarik	tarik	PROPN
eurjchem-208	1	61	el‐sayed	el‐saye	VERB
eurjchem-208	1	62	ali	ali	PROPN
eurjchem-208	1	63	*	*	PROPN
eurjchem-208	1	64	,	,	PUNCT
eurjchem-208	1	65	kamilia	kamilia	PROPN
eurjchem-208	1	66	mohamed	mohame	VERB
eurjchem-208	1	67	el‐mahdy	el‐mahdy	PROPN
eurjchem-208	1	68	and	and	CCONJ
eurjchem-208	1	69	somaia	somaia	PROPN
eurjchem-208	1	70	mohamed	mohamed	PROPN
eurjchem-208	1	71	abdel‐karim	abdel‐karim	PROPN
eurjchem-208	1	72	department	department	PROPN
eurjchem-208	1	73	of	of	ADP
eurjchem-208	1	74	chemistry	chemistry	NOUN
eurjchem-208	1	75	,	,	PUNCT
eurjchem-208	1	76	faculty	faculty	NOUN
eurjchem-208	1	77	of	of	ADP
eurjchem-208	1	78	education	education	NOUN
eurjchem-208	1	79	,	,	PUNCT
eurjchem-208	1	80	ain	ain	PROPN
eurjchem-208	1	81	shams	shams	PROPN
eurjchem-208	1	82	university	university	PROPN
eurjchem-208	1	83	,	,	PUNCT
eurjchem-208	1	84	roxy	roxy	PROPN
eurjchem-208	1	85	,	,	PUNCT
eurjchem-208	1	86	cairo	cairo	PROPN
eurjchem-208	1	87	,	,	PUNCT
eurjchem-208	1	88	eg‐11711	eg‐11711	PROPN
eurjchem-208	1	89	,	,	PUNCT
eurjchem-208	1	90	egypt	egypt	PROPN
eurjchem-208	1	91	*	*	PUNCT
eurjchem-208	1	92	corresponding	correspond	VERB
eurjchem-208	1	93	author	author	NOUN
eurjchem-208	1	94	at	at	ADP
eurjchem-208	1	95	:	:	PUNCT
eurjchem-208	1	96	department	department	NOUN
eurjchem-208	1	97	of	of	ADP
eurjchem-208	1	98	chemistry	chemistry	NOUN
eurjchem-208	1	99	,	,	PUNCT
eurjchem-208	1	100	faculty	faculty	NOUN
eurjchem-208	1	101	of	of	ADP
eurjchem-208	1	102	education	education	NOUN
eurjchem-208	1	103	,	,	PUNCT
eurjchem-208	1	104	ain	ain	PROPN
eurjchem-208	1	105	shams	shams	PROPN
eurjchem-208	1	106	university	university	PROPN
eurjchem-208	1	107	,	,	PUNCT
eurjchem-208	1	108	roxy	roxy	PROPN
eurjchem-208	1	109	,	,	PUNCT
eurjchem-208	1	110	cairo	cairo	PROPN
eurjchem-208	1	111	,	,	PUNCT
eurjchem-208	1	112	eg‐11711	eg‐11711	PROPN
eurjchem-208	1	113	,	,	PUNCT
eurjchem-208	1	114	egypt.tel	egypt.tel	X
eurjchem-208	1	115	.	.	PUNCT
eurjchem-208	1	116	:	:	PUNCT
eurjchem-208	2	1	+2.010.3730144	+2.010.3730144	ADV
eurjchem-208	2	2	;	;	PUNCT
eurjchem-208	2	3	fax	fax	NOUN
eurjchem-208	2	4	:	:	PUNCT
eurjchem-208	2	5	+2022581243	+2022581243	ADJ
eurjchem-208	2	6	.	.	PUNCT
eurjchem-208	2	7	e‐mail	e‐mail	PUNCT
eurjchem-208	3	1	address	address	NOUN
eurjchem-208	3	2	:	:	PUNCT
eurjchem-208	3	3	tarik_elsayed1975@yahoo.com	tarik_elsayed1975@yahoo.com	X
eurjchem-208	3	4	(	(	PUNCT
eurjchem-208	3	5	t.e	t.e	PROPN
eurjchem-208	3	6	.	.	PROPN
eurjchem-208	3	7	ali	ali	PROPN
eurjchem-208	3	8	)	)	PUNCT
eurjchem-208	3	9	.	.	PUNCT
eurjchem-208	4	1	article	article	NOUN
eurjchem-208	4	2	information	information	PROPN
eurjchem-208	4	3	abstract	abstract	ADV
eurjchem-208	4	4	received	receive	VERB
eurjchem-208	4	5	:	:	PUNCT
eurjchem-208	4	6	15	15	NUM
eurjchem-208	4	7	july	july	PROPN
eurjchem-208	4	8	2010	2010	NUM
eurjchem-208	4	9	received	receive	VERB
eurjchem-208	4	10	in	in	ADP
eurjchem-208	4	11	revised	revise	VERB
eurjchem-208	4	12	form	form	NOUN
eurjchem-208	4	13	:	:	PUNCT
eurjchem-208	4	14	10	10	NUM
eurjchem-208	4	15	august	august	PROPN
eurjchem-208	4	16	2010	2010	NUM
eurjchem-208	4	17	accepted	accept	VERB
eurjchem-208	4	18	:	:	PUNCT
eurjchem-208	4	19	16	16	NUM
eurjchem-208	4	20	august	august	PROPN
eurjchem-208	4	21	2010	2010	NUM
eurjchem-208	4	22	online	online	NOUN
eurjchem-208	4	23	:	:	PUNCT
eurjchem-208	4	24	31	31	NUM
eurjchem-208	4	25	march	march	NOUN
eurjchem-208	4	26	2011	2011	NUM
eurjchem-208	4	27	keywords	keyword	NOUN
eurjchem-208	4	28	vilsmeier‐haack	vilsmeier‐haack	VERB
eurjchem-208	4	29	reaction	reaction	NOUN
eurjchem-208	4	30	conditions	condition	NOUN
eurjchem-208	4	31	were	be	AUX
eurjchem-208	4	32	applied	apply	VERB
eurjchem-208	4	33	on	on	ADP
eurjchem-208	4	34	some	some	DET
eurjchem-208	4	35	methyl	methyl	NOUN
eurjchem-208	4	36	ketone	ketone	NOUN
eurjchem-208	4	37	aryl	aryl	NOUN
eurjchem-208	4	38	phosphonicdihydrazones	phosphonicdihydrazone	NOUN
eurjchem-208	4	39	to	to	PART
eurjchem-208	4	40	yield	yield	VERB
eurjchem-208	4	41	some	some	DET
eurjchem-208	4	42	interesting	interesting	ADJ
eurjchem-208	4	43	bis‐pyrazole	bis‐pyrazole	NOUN
eurjchem-208	4	44	derivatives	derivative	NOUN
eurjchem-208	4	45	containing	contain	VERB
eurjchem-208	4	46	a	a	DET
eurjchem-208	4	47	hydro‐phosphoryl	hydro‐phosphoryl	NOUN
eurjchem-208	4	48	unit	unit	NOUN
eurjchem-208	4	49	.	.	PUNCT
eurjchem-208	5	1	bis‐{4‐formyl‐3‐aryl‐1h‐pyrazol‐1‐yl}phosphine	bis‐{4‐formyl‐3‐aryl‐1h‐pyrazol‐1‐yl}phosphine	NOUN
eurjchem-208	5	2	oxides	oxide	NOUN
eurjchem-208	5	3	(	(	PUNCT
eurjchem-208	5	4	4a	4a	NUM
eurjchem-208	5	5	,	,	PUNCT
eurjchem-208	5	6	b	b	X
eurjchem-208	5	7	)	)	PUNCT
eurjchem-208	5	8	were	be	AUX
eurjchem-208	5	9	condensed	condense	VERB
eurjchem-208	5	10	with	with	ADP
eurjchem-208	5	11	some	some	DET
eurjchem-208	5	12	nucleophiles	nucleophile	NOUN
eurjchem-208	5	13	such	such	ADJ
eurjchem-208	5	14	as	as	ADP
eurjchem-208	5	15	aniline	aniline	NOUN
eurjchem-208	5	16	,	,	PUNCT
eurjchem-208	5	17	phenacyltriphenylphosphonium	phenacyltriphenylphosphonium	NOUN
eurjchem-208	5	18	bromide	bromide	NOUN
eurjchem-208	5	19	and	and	CCONJ
eurjchem-208	5	20	4‐phenylthiosemicarbazide	4‐phenylthiosemicarbazide	PROPN
eurjchem-208	5	21	followed	follow	VERB
eurjchem-208	5	22	by	by	ADP
eurjchem-208	5	23	treatment	treatment	NOUN
eurjchem-208	5	24	with	with	ADP
eurjchem-208	5	25	thioglycolic	thioglycolic	ADJ
eurjchem-208	5	26	acid	acid	NOUN
eurjchem-208	5	27	,	,	PUNCT
eurjchem-208	5	28	diethyl	diethyl	NOUN
eurjchem-208	5	29	phosphite	phosphite	NOUN
eurjchem-208	5	30	and/or	and/or	CCONJ
eurjchem-208	5	31	acetic	acetic	ADJ
eurjchem-208	5	32	anhydride	anhydride	NOUN
eurjchem-208	5	33	to	to	PART
eurjchem-208	5	34	yield	yield	VERB
eurjchem-208	5	35	a	a	DET
eurjchem-208	5	36	novel	novel	ADJ
eurjchem-208	5	37	class	class	NOUN
eurjchem-208	5	38	of	of	ADP
eurjchem-208	5	39	bis‐pyrazoles	bis‐pyrazoles	ADP
eurjchem-208	5	40	containing	contain	VERB
eurjchem-208	5	41	sulfur	sulfur	NOUN
eurjchem-208	5	42	and	and	CCONJ
eurjchem-208	5	43	phosphorus	phosphorus	NOUN
eurjchem-208	5	44	derivatives	derivative	NOUN
eurjchem-208	5	45	.	.	PUNCT
eurjchem-208	6	1	most	most	ADJ
eurjchem-208	6	2	of	of	ADP
eurjchem-208	6	3	the	the	DET
eurjchem-208	6	4	newly	newly	ADV
eurjchem-208	6	5	synthesized	synthesize	VERB
eurjchem-208	6	6	compounds	compound	NOUN
eurjchem-208	6	7	were	be	AUX
eurjchem-208	6	8	evaluated	evaluate	VERB
eurjchem-208	6	9	for	for	ADP
eurjchem-208	6	10	their	their	PRON
eurjchem-208	6	11	in	in	X
eurjchem-208	6	12	vitro	vitro	X
eurjchem-208	6	13	antimicrobial	antimicrobial	ADJ
eurjchem-208	6	14	activities	activity	NOUN
eurjchem-208	6	15	.	.	PUNCT
eurjchem-208	7	1	phosphonicdihydrazones	phosphonicdihydrazone	NOUN
eurjchem-208	7	2	hydro‐phosphoryl	hydro‐phosphoryl	NOUN
eurjchem-208	7	3	vilsmeier‐haack	vilsmeier‐haack	NOUN
eurjchem-208	7	4	reaction	reaction	NOUN
eurjchem-208	7	5	bis‐pyrazoles	bis‐pyrazoles	ADP
eurjchem-208	7	6	sulfur‐phosphorus	sulfur‐phosphorus	NOUN
eurjchem-208	7	7	heterocycles	heterocycle	NOUN
eurjchem-208	7	8	antimicrobial	antimicrobial	ADJ
eurjchem-208	7	9	activity	activity	NOUN
eurjchem-208	7	10	1	1	NUM
eurjchem-208	7	11	.	.	PUNCT
eurjchem-208	7	12	introduction	introduction	NOUN
eurjchem-208	7	13	pyrazole	pyrazole	NOUN
eurjchem-208	7	14	and	and	CCONJ
eurjchem-208	7	15	its	its	PRON
eurjchem-208	7	16	derivatives	derivative	NOUN
eurjchem-208	7	17	represent	represent	VERB
eurjchem-208	7	18	one	one	NUM
eurjchem-208	7	19	of	of	ADP
eurjchem-208	7	20	the	the	DET
eurjchem-208	7	21	most	most	ADV
eurjchem-208	7	22	active	active	ADJ
eurjchem-208	7	23	classes	class	NOUN
eurjchem-208	7	24	of	of	ADP
eurjchem-208	7	25	compounds	compound	NOUN
eurjchem-208	7	26	possessing	possess	VERB
eurjchem-208	7	27	a	a	DET
eurjchem-208	7	28	wide	wide	ADJ
eurjchem-208	7	29	spectrum	spectrum	NOUN
eurjchem-208	7	30	of	of	ADP
eurjchem-208	7	31	biological	biological	ADJ
eurjchem-208	7	32	activities	activity	NOUN
eurjchem-208	7	33	including	include	VERB
eurjchem-208	7	34	antibacterial	antibacterial	ADJ
eurjchem-208	7	35	[	[	X
eurjchem-208	7	36	1,2	1,2	NUM
eurjchem-208	7	37	]	]	PUNCT
eurjchem-208	7	38	,	,	PUNCT
eurjchem-208	7	39	antifungal	antifungal	PROPN
eurjchem-208	8	1	[	[	X
eurjchem-208	8	2	3,4	3,4	NUM
eurjchem-208	8	3	]	]	PUNCT
eurjchem-208	8	4	,	,	PUNCT
eurjchem-208	8	5	herbicidal	herbicidal	NOUN
eurjchem-208	8	6	[	[	X
eurjchem-208	8	7	5	5	NUM
eurjchem-208	8	8	]	]	PUNCT
eurjchem-208	8	9	,	,	PUNCT
eurjchem-208	8	10	insecticidal	insecticidal	NOUN
eurjchem-208	8	11	[	[	X
eurjchem-208	8	12	6	6	NUM
eurjchem-208	8	13	]	]	PUNCT
eurjchem-208	8	14	,	,	PUNCT
eurjchem-208	8	15	and	and	CCONJ
eurjchem-208	8	16	other	other	ADJ
eurjchem-208	8	17	biological	biological	ADJ
eurjchem-208	8	18	activities	activity	NOUN
eurjchem-208	8	19	[	[	X
eurjchem-208	8	20	7	7	NUM
eurjchem-208	8	21	]	]	PUNCT
eurjchem-208	8	22	.	.	PUNCT
eurjchem-208	9	1	up	up	ADV
eurjchem-208	9	2	till	till	SCONJ
eurjchem-208	9	3	now	now	ADV
eurjchem-208	9	4	,	,	PUNCT
eurjchem-208	9	5	a	a	DET
eurjchem-208	9	6	great	great	ADJ
eurjchem-208	9	7	variety	variety	NOUN
eurjchem-208	9	8	of	of	ADP
eurjchem-208	9	9	these	these	DET
eurjchem-208	9	10	kinds	kind	NOUN
eurjchem-208	9	11	of	of	ADP
eurjchem-208	9	12	compounds	compound	NOUN
eurjchem-208	9	13	have	have	AUX
eurjchem-208	9	14	been	be	AUX
eurjchem-208	9	15	synthesized	synthesize	VERB
eurjchem-208	9	16	,	,	PUNCT
eurjchem-208	9	17	among	among	ADP
eurjchem-208	9	18	which	which	PRON
eurjchem-208	9	19	some	some	DET
eurjchem-208	9	20	commercial	commercial	ADJ
eurjchem-208	9	21	pesticides	pesticide	NOUN
eurjchem-208	9	22	have	have	AUX
eurjchem-208	9	23	been	be	AUX
eurjchem-208	9	24	developed	develop	VERB
eurjchem-208	9	25	including	include	VERB
eurjchem-208	9	26	fripronil	fripronil	NOUN
eurjchem-208	9	27	(	(	PUNCT
eurjchem-208	9	28	mb46030	mb46030	PROPN
eurjchem-208	9	29	)	)	PUNCT
eurjchem-208	10	1	[	[	X
eurjchem-208	10	2	8	8	NUM
eurjchem-208	10	3	]	]	PUNCT
eurjchem-208	10	4	,	,	PUNCT
eurjchem-208	10	5	et‐751	et‐751	PROPN
eurjchem-208	11	1	[	[	X
eurjchem-208	11	2	9	9	NUM
eurjchem-208	11	3	]	]	PUNCT
eurjchem-208	11	4	,	,	PUNCT
eurjchem-208	11	5	and	and	CCONJ
eurjchem-208	11	6	pyrazolate	pyrazolate	NOUN
eurjchem-208	11	7	(	(	PUNCT
eurjchem-208	11	8	a‐544	a‐544	NOUN
eurjchem-208	11	9	)	)	PUNCT
eurjchem-208	11	10	[	[	X
eurjchem-208	11	11	10	10	NUM
eurjchem-208	11	12	]	]	PUNCT
eurjchem-208	11	13	.	.	PUNCT
eurjchem-208	12	1	on	on	ADP
eurjchem-208	12	2	the	the	DET
eurjchem-208	12	3	other	other	ADJ
eurjchem-208	12	4	hand	hand	NOUN
eurjchem-208	12	5	,	,	PUNCT
eurjchem-208	12	6	organophosphorus	organophosphorus	NOUN
eurjchem-208	12	7	compounds	compound	NOUN
eurjchem-208	12	8	possess	possess	VERB
eurjchem-208	12	9	insecticidal	insecticidal	NOUN
eurjchem-208	12	10	,	,	PUNCT
eurjchem-208	12	11	pesticidal	pesticidal	NOUN
eurjchem-208	12	12	,	,	PUNCT
eurjchem-208	12	13	acaricidal	acaricidal	NOUN
eurjchem-208	12	14	and	and	CCONJ
eurjchem-208	12	15	antimicrobial	antimicrobial	ADJ
eurjchem-208	12	16	properties	property	NOUN
eurjchem-208	12	17	[	[	X
eurjchem-208	12	18	11‐15	11‐15	NUM
eurjchem-208	12	19	]	]	PUNCT
eurjchem-208	12	20	.	.	PUNCT
eurjchem-208	13	1	these	these	DET
eurjchem-208	13	2	compounds	compound	NOUN
eurjchem-208	13	3	exert	exert	VERB
eurjchem-208	13	4	their	their	PRON
eurjchem-208	13	5	biological	biological	ADJ
eurjchem-208	13	6	action	action	NOUN
eurjchem-208	13	7	on	on	ADP
eurjchem-208	13	8	arthropods	arthropod	NOUN
eurjchem-208	13	9	by	by	ADP
eurjchem-208	13	10	attacking	attack	VERB
eurjchem-208	13	11	the	the	DET
eurjchem-208	13	12	system	system	NOUN
eurjchem-208	13	13	of	of	ADP
eurjchem-208	13	14	neural	neural	ADJ
eurjchem-208	13	15	transmission	transmission	NOUN
eurjchem-208	13	16	and	and	CCONJ
eurjchem-208	13	17	inhibiting	inhibit	VERB
eurjchem-208	13	18	the	the	DET
eurjchem-208	13	19	function	function	NOUN
eurjchem-208	13	20	of	of	ADP
eurjchem-208	13	21	acetyl	acetyl	NOUN
eurjchem-208	13	22	cholinesterase	cholinesterase	NOUN
eurjchem-208	14	1	[	[	X
eurjchem-208	14	2	16,17	16,17	NUM
eurjchem-208	14	3	]	]	PUNCT
eurjchem-208	14	4	.	.	PUNCT
eurjchem-208	15	1	in	in	ADP
eurjchem-208	15	2	particular	particular	ADJ
eurjchem-208	15	3	,	,	PUNCT
eurjchem-208	15	4	organophosphorus	organophosphorus	NOUN
eurjchem-208	15	5	compounds	compound	NOUN
eurjchem-208	15	6	including	include	VERB
eurjchem-208	15	7	hydro‐	hydro‐	X
eurjchem-208	15	8	phosphoryl	phosphoryl	PROPN
eurjchem-208	15	9	group	group	PROPN
eurjchem-208	15	10	(	(	PUNCT
eurjchem-208	15	11	h−p	h−p	NOUN
eurjchem-208	15	12	=	=	SYM
eurjchem-208	15	13	o	o	NOUN
eurjchem-208	15	14	)	)	PUNCT
eurjchem-208	15	15	are	be	AUX
eurjchem-208	15	16	widely	widely	ADV
eurjchem-208	15	17	used	use	VERB
eurjchem-208	15	18	in	in	ADP
eurjchem-208	15	19	industry	industry	NOUN
eurjchem-208	15	20	,	,	PUNCT
eurjchem-208	15	21	agriculture	agriculture	NOUN
eurjchem-208	15	22	and	and	CCONJ
eurjchem-208	15	23	medicine	medicine	NOUN
eurjchem-208	15	24	.	.	PUNCT
eurjchem-208	16	1	it	it	PRON
eurjchem-208	16	2	is	be	AUX
eurjchem-208	16	3	interesting	interesting	ADJ
eurjchem-208	16	4	that	that	SCONJ
eurjchem-208	16	5	many	many	ADJ
eurjchem-208	16	6	hydro‐	hydro‐	X
eurjchem-208	16	7	phosphoryl	phosphoryl	PROPN
eurjchem-208	16	8	compounds	compound	NOUN
eurjchem-208	16	9	are	be	AUX
eurjchem-208	16	10	also	also	ADV
eurjchem-208	16	11	used	use	VERB
eurjchem-208	16	12	as	as	ADP
eurjchem-208	16	13	complexing	complexe	VERB
eurjchem-208	16	14	and	and	CCONJ
eurjchem-208	16	15	extracting	extract	VERB
eurjchem-208	16	16	agents	agent	NOUN
eurjchem-208	16	17	,	,	PUNCT
eurjchem-208	16	18	as	as	ADV
eurjchem-208	16	19	well	well	ADV
eurjchem-208	16	20	as	as	ADP
eurjchem-208	16	21	corrosion	corrosion	NOUN
eurjchem-208	16	22	and	and	CCONJ
eurjchem-208	16	23	saline	saline	ADJ
eurjchem-208	16	24	deposition	deposition	NOUN
eurjchem-208	16	25	inhibitors	inhibitor	NOUN
eurjchem-208	16	26	[	[	X
eurjchem-208	16	27	18,19	18,19	NUM
eurjchem-208	16	28	]	]	PUNCT
eurjchem-208	16	29	.	.	PUNCT
eurjchem-208	17	1	the	the	DET
eurjchem-208	17	2	connection	connection	NOUN
eurjchem-208	17	3	of	of	ADP
eurjchem-208	17	4	a	a	DET
eurjchem-208	17	5	heterocyclic	heterocyclic	ADJ
eurjchem-208	17	6	moiety	moiety	NOUN
eurjchem-208	17	7	with	with	ADP
eurjchem-208	17	8	organo‐phosphorus	organo‐phosphorus	PROPN
eurjchem-208	17	9	compounds	compound	NOUN
eurjchem-208	17	10	further	far	ADV
eurjchem-208	17	11	may	may	AUX
eurjchem-208	17	12	enhance	enhance	VERB
eurjchem-208	17	13	their	their	PRON
eurjchem-208	17	14	biological	biological	ADJ
eurjchem-208	17	15	activities	activity	NOUN
eurjchem-208	17	16	.	.	PUNCT
eurjchem-208	18	1	in	in	ADP
eurjchem-208	18	2	continuation	continuation	NOUN
eurjchem-208	18	3	of	of	ADP
eurjchem-208	18	4	our	our	PRON
eurjchem-208	18	5	research	research	NOUN
eurjchem-208	18	6	work	work	NOUN
eurjchem-208	18	7	on	on	ADP
eurjchem-208	18	8	the	the	DET
eurjchem-208	18	9	synthesis	synthesis	NOUN
eurjchem-208	18	10	of	of	ADP
eurjchem-208	18	11	bioactive	bioactive	ADJ
eurjchem-208	18	12	phosphorus	phosphorus	NOUN
eurjchem-208	18	13	containing	contain	VERB
eurjchem-208	18	14	heterocycles	heterocycle	NOUN
eurjchem-208	18	15	[	[	X
eurjchem-208	18	16	13,15,20‐22	13,15,20‐22	X
eurjchem-208	18	17	]	]	X
eurjchem-208	18	18	,	,	PUNCT
eurjchem-208	18	19	it	it	PRON
eurjchem-208	18	20	was	be	AUX
eurjchem-208	18	21	considered	consider	VERB
eurjchem-208	18	22	valuable	valuable	ADJ
eurjchem-208	18	23	to	to	PART
eurjchem-208	18	24	integrate	integrate	VERB
eurjchem-208	18	25	hydrophosphoryl	hydrophosphoryl	ADJ
eurjchem-208	18	26	unit	unit	NOUN
eurjchem-208	18	27	and	and	CCONJ
eurjchem-208	18	28	pyrazole	pyrazole	NOUN
eurjchem-208	18	29	rings	ring	NOUN
eurjchem-208	18	30	together	together	ADV
eurjchem-208	18	31	in	in	ADP
eurjchem-208	18	32	a	a	DET
eurjchem-208	18	33	molecular	molecular	ADJ
eurjchem-208	18	34	frame	frame	NOUN
eurjchem-208	18	35	to	to	PART
eurjchem-208	18	36	see	see	VERB
eurjchem-208	18	37	the	the	DET
eurjchem-208	18	38	additive	additive	ADJ
eurjchem-208	18	39	effect	effect	NOUN
eurjchem-208	18	40	of	of	ADP
eurjchem-208	18	41	these	these	DET
eurjchem-208	18	42	novel	novel	NOUN
eurjchem-208	18	43	frames	frame	NOUN
eurjchem-208	18	44	towards	towards	ADP
eurjchem-208	18	45	the	the	DET
eurjchem-208	18	46	antimicrobial	antimicrobial	ADJ
eurjchem-208	18	47	activity	activity	NOUN
eurjchem-208	18	48	.	.	PUNCT
eurjchem-208	19	1	2	2	X
eurjchem-208	19	2	.	.	X
eurjchem-208	19	3	experimental	experimental	ADJ
eurjchem-208	19	4	2.1	2.1	NUM
eurjchem-208	19	5	.	.	PUNCT
eurjchem-208	20	1	instrumentation	instrumentation	NOUN
eurjchem-208	20	2	the	the	DET
eurjchem-208	20	3	melting	melting	NOUN
eurjchem-208	20	4	point	point	NOUN
eurjchem-208	20	5	was	be	AUX
eurjchem-208	20	6	determined	determine	VERB
eurjchem-208	20	7	in	in	ADP
eurjchem-208	20	8	an	an	DET
eurjchem-208	20	9	open	open	ADJ
eurjchem-208	20	10	capillary	capillary	ADJ
eurjchem-208	20	11	tube	tube	NOUN
eurjchem-208	20	12	on	on	ADP
eurjchem-208	20	13	a	a	DET
eurjchem-208	20	14	digital	digital	ADJ
eurjchem-208	20	15	stuart	stuart	PROPN
eurjchem-208	20	16	smp‐3	smp‐3	PROPN
eurjchem-208	20	17	apparatus	apparatus	PROPN
eurjchem-208	20	18	.	.	PUNCT
eurjchem-208	21	1	infrared	infrared	PROPN
eurjchem-208	21	2	spectra	spectra	PROPN
eurjchem-208	21	3	were	be	AUX
eurjchem-208	21	4	measured	measure	VERB
eurjchem-208	21	5	on	on	ADP
eurjchem-208	21	6	perkin‐elmer	perkin‐elmer	PROPN
eurjchem-208	21	7	293	293	NUM
eurjchem-208	21	8	spectrophotometer	spectrophotometer	NOUN
eurjchem-208	21	9	,	,	PUNCT
eurjchem-208	21	10	using	use	VERB
eurjchem-208	21	11	kbr	kbr	PROPN
eurjchem-208	21	12	disks	disk	NOUN
eurjchem-208	21	13	.	.	PUNCT
eurjchem-208	22	1	1h	1h	NUM
eurjchem-208	22	2	nmr	nmr	PROPN
eurjchem-208	22	3	spectra	spectra	NOUN
eurjchem-208	22	4	were	be	AUX
eurjchem-208	22	5	measured	measure	VERB
eurjchem-208	22	6	on	on	ADP
eurjchem-208	22	7	gemini‐200	gemini‐200	PROPN
eurjchem-208	22	8	spectro‐	spectro‐	NOUN
eurjchem-208	22	9	meter	meter	NOUN
eurjchem-208	22	10	(	(	PUNCT
eurjchem-208	22	11	200	200	NUM
eurjchem-208	22	12	mhz	mhz	NOUN
eurjchem-208	22	13	)	)	PUNCT
eurjchem-208	22	14	,	,	PUNCT
eurjchem-208	22	15	using	use	VERB
eurjchem-208	22	16	dmso‐d6	dmso‐d6	PROPN
eurjchem-208	22	17	as	as	ADP
eurjchem-208	22	18	a	a	DET
eurjchem-208	22	19	solvent	solvent	NOUN
eurjchem-208	22	20	and	and	CCONJ
eurjchem-208	22	21	tms	tms	PROPN
eurjchem-208	22	22	(	(	PUNCT
eurjchem-208	22	23	δ	δ	PROPN
eurjchem-208	22	24	)	)	PUNCT
eurjchem-208	22	25	as	as	ADP
eurjchem-208	22	26	the	the	DET
eurjchem-208	22	27	internal	internal	ADJ
eurjchem-208	22	28	standard	standard	NOUN
eurjchem-208	22	29	.	.	PUNCT
eurjchem-208	22	30	13c	13c	NOUN
eurjchem-208	22	31	nmr	nmr	NOUN
eurjchem-208	22	32	spectra	spectra	NOUN
eurjchem-208	22	33	were	be	AUX
eurjchem-208	22	34	measured	measure	VERB
eurjchem-208	22	35	on	on	ADP
eurjchem-208	22	36	mercury‐300bb	mercury‐300bb	PROPN
eurjchem-208	22	37	(	(	PUNCT
eurjchem-208	22	38	75	75	NUM
eurjchem-208	22	39	mhz	mhz	NOUN
eurjchem-208	22	40	)	)	PUNCT
eurjchem-208	22	41	,	,	PUNCT
eurjchem-208	22	42	using	use	VERB
eurjchem-208	22	43	dmso‐d6	dmso‐d6	PROPN
eurjchem-208	22	44	as	as	ADP
eurjchem-208	22	45	a	a	DET
eurjchem-208	22	46	solvent	solvent	NOUN
eurjchem-208	22	47	and	and	CCONJ
eurjchem-208	22	48	tms	tms	PROPN
eurjchem-208	22	49	(	(	PUNCT
eurjchem-208	22	50	δ	δ	PROPN
eurjchem-208	22	51	)	)	PUNCT
eurjchem-208	22	52	as	as	ADP
eurjchem-208	22	53	the	the	DET
eurjchem-208	22	54	internal	internal	ADJ
eurjchem-208	22	55	standard	standard	NOUN
eurjchem-208	22	56	.	.	PUNCT
eurjchem-208	23	1	31p	31p	PROPN
eurjchem-208	23	2	nmr	nmr	NOUN
eurjchem-208	23	3	spectra	spectra	NOUN
eurjchem-208	23	4	were	be	AUX
eurjchem-208	23	5	registered	register	VERB
eurjchem-208	23	6	on	on	ADP
eurjchem-208	23	7	a	a	DET
eurjchem-208	23	8	varian	varian	PROPN
eurjchem-208	23	9	inova	inova	PROPN
eurjchem-208	23	10	500	500	NUM
eurjchem-208	23	11	mhz	mhz	NOUN
eurjchem-208	23	12	spectrometer	spectrometer	NOUN
eurjchem-208	23	13	at	at	ADP
eurjchem-208	23	14	room	room	NOUN
eurjchem-208	23	15	temperature	temperature	NOUN
eurjchem-208	23	16	using	use	VERB
eurjchem-208	23	17	dmso‐d6	dmso‐d6	PROPN
eurjchem-208	23	18	as	as	ADP
eurjchem-208	23	19	a	a	DET
eurjchem-208	23	20	solvent	solvent	NOUN
eurjchem-208	23	21	and	and	CCONJ
eurjchem-208	23	22	tms	tms	PROPN
eurjchem-208	23	23	as	as	ADP
eurjchem-208	23	24	internal	internal	ADJ
eurjchem-208	23	25	standard	standard	NOUN
eurjchem-208	23	26	and	and	CCONJ
eurjchem-208	23	27	85	85	NUM
eurjchem-208	23	28	%	%	NOUN
eurjchem-208	23	29	h3po4	h3po4	NOUN
eurjchem-208	23	30	as	as	ADP
eurjchem-208	23	31	external	external	ADJ
eurjchem-208	23	32	reference	reference	NOUN
eurjchem-208	23	33	.	.	PUNCT
eurjchem-208	24	1	mass	mass	PROPN
eurjchem-208	24	2	spectra	spectra	PROPN
eurjchem-208	24	3	recorded	record	VERB
eurjchem-208	24	4	on	on	ADP
eurjchem-208	24	5	a	a	DET
eurjchem-208	24	6	gas	gas	NOUN
eurjchem-208	24	7	chromatographic	chromatographic	ADJ
eurjchem-208	24	8	gcmsqp	gcmsqp	NOUN
eurjchem-208	24	9	1000	1000	NUM
eurjchem-208	24	10	ex	ex	PRON
eurjchem-208	24	11	shimadzu	shimadzu	ADJ
eurjchem-208	24	12	instrument	instrument	NOUN
eurjchem-208	24	13	at	at	ADP
eurjchem-208	24	14	70	70	NUM
eurjchem-208	24	15	ev	ev	NOUN
eurjchem-208	24	16	.	.	PROPN
eurjchem-208	24	17	elemental	elemental	ADJ
eurjchem-208	24	18	microanalyses	microanalysis	NOUN
eurjchem-208	24	19	were	be	AUX
eurjchem-208	24	20	performed	perform	VERB
eurjchem-208	24	21	at	at	ADP
eurjchem-208	24	22	micro‐	micro‐	NOUN
eurjchem-208	24	23	analysis	analysis	NOUN
eurjchem-208	24	24	center	center	NOUN
eurjchem-208	24	25	in	in	ADP
eurjchem-208	24	26	national	national	ADJ
eurjchem-208	24	27	research	research	NOUN
eurjchem-208	24	28	center	center	PROPN
eurjchem-208	24	29	,	,	PUNCT
eurjchem-208	24	30	giza	giza	PROPN
eurjchem-208	24	31	.	.	PUNCT
eurjchem-208	25	1	the	the	DET
eurjchem-208	25	2	purity	purity	NOUN
eurjchem-208	25	3	of	of	ADP
eurjchem-208	25	4	the	the	DET
eurjchem-208	25	5	synthesized	synthesize	VERB
eurjchem-208	25	6	compounds	compound	NOUN
eurjchem-208	25	7	was	be	AUX
eurjchem-208	25	8	checked	check	VERB
eurjchem-208	25	9	by	by	ADP
eurjchem-208	25	10	thin	thin	ADJ
eurjchem-208	25	11	layer	layer	NOUN
eurjchem-208	25	12	chromatography	chromatography	NOUN
eurjchem-208	25	13	(	(	PUNCT
eurjchem-208	25	14	tlc	tlc	NOUN
eurjchem-208	25	15	)	)	PUNCT
eurjchem-208	25	16	.	.	PUNCT
eurjchem-208	26	1	2.2	2.2	NUM
eurjchem-208	26	2	.	.	PUNCT
eurjchem-208	26	3	synthesis	synthesis	NOUN
eurjchem-208	26	4	2.2.1	2.2.1	NUM
eurjchem-208	26	5	.	.	PUNCT
eurjchem-208	26	6	preparation	preparation	NOUN
eurjchem-208	26	7	of	of	ADP
eurjchem-208	26	8	phosphonicdihydrazide	phosphonicdihydrazide	NOUN
eurjchem-208	26	9	(	(	PUNCT
eurjchem-208	26	10	1	1	NUM
eurjchem-208	26	11	)	)	PUNCT
eurjchem-208	26	12	a	a	DET
eurjchem-208	26	13	mixture	mixture	NOUN
eurjchem-208	26	14	of	of	ADP
eurjchem-208	26	15	hydrazine	hydrazine	NOUN
eurjchem-208	26	16	hydrate	hydrate	NOUN
eurjchem-208	26	17	99	99	NUM
eurjchem-208	26	18	%	%	NOUN
eurjchem-208	26	19	(	(	PUNCT
eurjchem-208	26	20	0.1	0.1	NUM
eurjchem-208	26	21	mol	mol	NOUN
eurjchem-208	26	22	,	,	PUNCT
eurjchem-208	26	23	5	5	NUM
eurjchem-208	26	24	cm3	cm3	NOUN
eurjchem-208	26	25	)	)	PUNCT
eurjchem-208	26	26	and	and	CCONJ
eurjchem-208	26	27	diethyl	diethyl	NOUN
eurjchem-208	26	28	phosphite	phosphite	NOUN
eurjchem-208	26	29	(	(	PUNCT
eurjchem-208	26	30	0.05	0.05	NUM
eurjchem-208	26	31	mol	mol	NOUN
eurjchem-208	26	32	,	,	PUNCT
eurjchem-208	26	33	7	7	NUM
eurjchem-208	26	34	cm3	cm3	NOUN
eurjchem-208	26	35	)	)	PUNCT
eurjchem-208	26	36	was	be	AUX
eurjchem-208	26	37	heated	heat	VERB
eurjchem-208	26	38	under	under	ADP
eurjchem-208	26	39	reflux	reflux	NOUN
eurjchem-208	26	40	at	at	ADP
eurjchem-208	26	41	70‐80	70‐80	NUM
eurjchem-208	26	42	oc	oc	NOUN
eurjchem-208	26	43	for	for	ADP
eurjchem-208	26	44	two	two	NUM
eurjchem-208	26	45	hours	hour	NOUN
eurjchem-208	26	46	.	.	PUNCT
eurjchem-208	27	1	the	the	DET
eurjchem-208	27	2	reaction	reaction	NOUN
eurjchem-208	27	3	mixture	mixture	NOUN
eurjchem-208	27	4	was	be	AUX
eurjchem-208	27	5	cooled	cool	VERB
eurjchem-208	27	6	in	in	ADP
eurjchem-208	27	7	an	an	DET
eurjchem-208	27	8	ice	ice	NOUN
eurjchem-208	27	9	bath	bath	NOUN
eurjchem-208	27	10	for	for	ADP
eurjchem-208	27	11	30	30	NUM
eurjchem-208	27	12	minutes	minute	NOUN
eurjchem-208	27	13	.	.	PUNCT
eurjchem-208	28	1	the	the	DET
eurjchem-208	28	2	formed	form	VERB
eurjchem-208	28	3	solid	solid	NOUN
eurjchem-208	28	4	was	be	AUX
eurjchem-208	28	5	filtered	filter	VERB
eurjchem-208	28	6	off	off	ADP
eurjchem-208	28	7	and	and	CCONJ
eurjchem-208	28	8	washed	wash	VERB
eurjchem-208	28	9	with	with	ADP
eurjchem-208	28	10	absolute	absolute	ADJ
eurjchem-208	28	11	ethanol	ethanol	NOUN
eurjchem-208	28	12	(	(	PUNCT
eurjchem-208	28	13	10	10	NUM
eurjchem-208	28	14	cm3	cm3	NOUN
eurjchem-208	28	15	)	)	PUNCT
eurjchem-208	28	16	.	.	PUNCT
eurjchem-208	29	1	the	the	DET
eurjchem-208	29	2	filtrate	filtrate	NOUN
eurjchem-208	29	3	was	be	AUX
eurjchem-208	29	4	concentrated	concentrate	VERB
eurjchem-208	29	5	to	to	ADP
eurjchem-208	29	6	its	its	PRON
eurjchem-208	29	7	third	third	ADJ
eurjchem-208	29	8	volume	volume	NOUN
eurjchem-208	29	9	under	under	ADP
eurjchem-208	29	10	reduced	reduce	VERB
eurjchem-208	29	11	pressure	pressure	NOUN
eurjchem-208	29	12	and	and	CCONJ
eurjchem-208	29	13	cooled	cool	VERB
eurjchem-208	29	14	in	in	ADP
eurjchem-208	29	15	an	an	DET
eurjchem-208	29	16	ice	ice	NOUN
eurjchem-208	29	17	bath	bath	NOUN
eurjchem-208	29	18	for	for	ADP
eurjchem-208	29	19	one	one	NUM
eurjchem-208	29	20	hour	hour	NOUN
eurjchem-208	29	21	.	.	PUNCT
eurjchem-208	30	1	the	the	DET
eurjchem-208	30	2	white	white	PROPN
eurjchem-208	30	3	solid	solid	NOUN
eurjchem-208	30	4	was	be	AUX
eurjchem-208	30	5	filtered	filter	VERB
eurjchem-208	30	6	off	off	ADP
eurjchem-208	30	7	and	and	CCONJ
eurjchem-208	30	8	dried	dry	VERB
eurjchem-208	30	9	.	.	PUNCT
eurjchem-208	31	1	total	total	ADJ
eurjchem-208	31	2	yield	yield	NOUN
eurjchem-208	31	3	:	:	PUNCT
eurjchem-208	31	4	80	80	NUM
eurjchem-208	31	5	%	%	NOUN
eurjchem-208	31	6	;	;	PUNCT
eurjchem-208	31	7	m.p	m.p	PROPN
eurjchem-208	31	8	.	.	PROPN
eurjchem-208	31	9	:	:	PUNCT
eurjchem-208	31	10	98‐99	98‐99	NUM
eurjchem-208	31	11	oc	oc	NOUN
eurjchem-208	31	12	(	(	PUNCT
eurjchem-208	31	13	lit	lit	ADJ
eurjchem-208	31	14	.	.	PUNCT
eurjchem-208	32	1	92‐94)[23	92‐94)[23	PROPN
eurjchem-208	32	2	]	]	X
eurjchem-208	32	3	.	.	PUNCT
eurjchem-208	33	1	26	26	NUM
eurjchem-208	33	2	abdel‐aziz	abdel‐aziz	INTJ
eurjchem-208	33	3	et	et	PROPN
eurjchem-208	33	4	al	al	PROPN
eurjchem-208	33	5	.	.	PUNCT
eurjchem-208	33	6	/	/	SYM
eurjchem-208	33	7	european	european	PROPN
eurjchem-208	33	8	journal	journal	PROPN
eurjchem-208	33	9	of	of	ADP
eurjchem-208	33	10	chemistry	chemistry	NOUN
eurjchem-208	33	11	2	2	NUM
eurjchem-208	33	12	(	(	PUNCT
eurjchem-208	33	13	1	1	NUM
eurjchem-208	33	14	)	)	PUNCT
eurjchem-208	33	15	(	(	PUNCT
eurjchem-208	33	16	2011	2011	NUM
eurjchem-208	33	17	)	)	PUNCT
eurjchem-208	33	18	25‐35	25‐35	NUM
eurjchem-208	33	19	2.2.2	2.2.2	NUM
eurjchem-208	33	20	.	.	PUNCT
eurjchem-208	33	21	general	general	ADJ
eurjchem-208	33	22	procedure	procedure	NOUN
eurjchem-208	33	23	for	for	ADP
eurjchem-208	33	24	preparation	preparation	NOUN
eurjchem-208	33	25	of	of	ADP
eurjchem-208	33	26	phosphonic	phosphonic	ADJ
eurjchem-208	33	27	dihydrazones	dihydrazone	NOUN
eurjchem-208	33	28	(	(	PUNCT
eurjchem-208	33	29	3a‐d	3a‐d	ADV
eurjchem-208	33	30	)	)	PUNCT
eurjchem-208	33	31	a	a	DET
eurjchem-208	33	32	mixture	mixture	NOUN
eurjchem-208	33	33	of	of	ADP
eurjchem-208	33	34	phosphonicdihydrazide	phosphonicdihydrazide	NOUN
eurjchem-208	33	35	(	(	PUNCT
eurjchem-208	33	36	1	1	NUM
eurjchem-208	33	37	)	)	PUNCT
eurjchem-208	33	38	(	(	PUNCT
eurjchem-208	33	39	0.01	0.01	NUM
eurjchem-208	33	40	mol	mol	NOUN
eurjchem-208	33	41	,	,	PUNCT
eurjchem-208	33	42	1.1	1.1	NUM
eurjchem-208	33	43	g	g	NOUN
eurjchem-208	33	44	)	)	PUNCT
eurjchem-208	33	45	and	and	CCONJ
eurjchem-208	33	46	acetophenone	acetophenone	NOUN
eurjchem-208	33	47	derivatives	derivative	NOUN
eurjchem-208	33	48	namely	namely	ADV
eurjchem-208	33	49	,	,	PUNCT
eurjchem-208	33	50	acetophenone	acetophenone	PROPN
eurjchem-208	33	51	(	(	PUNCT
eurjchem-208	33	52	2a	2a	NUM
eurjchem-208	33	53	)	)	PUNCT
eurjchem-208	33	54	,	,	PUNCT
eurjchem-208	33	55	4`‐	4`‐	PROPN
eurjchem-208	33	56	acetyl‐biphenyl	acetyl‐biphenyl	NOUN
eurjchem-208	33	57	(	(	PUNCT
eurjchem-208	33	58	2b	2b	NUM
eurjchem-208	33	59	)	)	PUNCT
eurjchem-208	33	60	,	,	PUNCT
eurjchem-208	33	61	2‐hydroxyacetophenone	2‐hydroxyacetophenone	NUM
eurjchem-208	33	62	(	(	PUNCT
eurjchem-208	33	63	2c	2c	NUM
eurjchem-208	33	64	)	)	PUNCT
eurjchem-208	33	65	and/or	and/or	CCONJ
eurjchem-208	33	66	3‐	3‐	NUM
eurjchem-208	33	67	acetyl‐2‐methylchromone	acetyl‐2‐methylchromone	NUM
eurjchem-208	33	68	(	(	PUNCT
eurjchem-208	33	69	2d	2d	NUM
eurjchem-208	33	70	)	)	PUNCT
eurjchem-208	33	71	(	(	PUNCT
eurjchem-208	33	72	0.02	0.02	NUM
eurjchem-208	33	73	mol	mol	NOUN
eurjchem-208	33	74	)	)	PUNCT
eurjchem-208	33	75	in	in	ADP
eurjchem-208	33	76	absolute	absolute	ADJ
eurjchem-208	33	77	ethanol	ethanol	NOUN
eurjchem-208	33	78	(	(	PUNCT
eurjchem-208	33	79	20	20	NUM
eurjchem-208	33	80	cm3	cm3	NOUN
eurjchem-208	33	81	)	)	PUNCT
eurjchem-208	33	82	in	in	ADP
eurjchem-208	33	83	the	the	DET
eurjchem-208	33	84	presence	presence	NOUN
eurjchem-208	33	85	of	of	ADP
eurjchem-208	33	86	few	few	ADJ
eurjchem-208	33	87	drops	drop	NOUN
eurjchem-208	33	88	of	of	ADP
eurjchem-208	33	89	concentrated	concentrated	ADJ
eurjchem-208	33	90	sulfuric	sulfuric	NOUN
eurjchem-208	33	91	acid	acid	NOUN
eurjchem-208	33	92	,	,	PUNCT
eurjchem-208	33	93	was	be	AUX
eurjchem-208	33	94	refluxed	refluxe	VERB
eurjchem-208	33	95	for	for	ADP
eurjchem-208	33	96	4	4	NUM
eurjchem-208	33	97	h.	h.	NOUN
eurjchem-208	33	98	the	the	DET
eurjchem-208	33	99	reaction	reaction	NOUN
eurjchem-208	33	100	mixture	mixture	NOUN
eurjchem-208	33	101	was	be	AUX
eurjchem-208	33	102	cooled	cool	VERB
eurjchem-208	33	103	;	;	PUNCT
eurjchem-208	33	104	the	the	DET
eurjchem-208	33	105	resulting	result	VERB
eurjchem-208	33	106	precipitate	precipitate	NOUN
eurjchem-208	33	107	was	be	AUX
eurjchem-208	33	108	filtered	filter	VERB
eurjchem-208	33	109	off	off	ADP
eurjchem-208	33	110	and	and	CCONJ
eurjchem-208	33	111	crystallized	crystallize	VERB
eurjchem-208	33	112	from	from	ADP
eurjchem-208	33	113	the	the	DET
eurjchem-208	33	114	proper	proper	ADJ
eurjchem-208	33	115	solvent	solvent	NOUN
eurjchem-208	33	116	to	to	PART
eurjchem-208	33	117	give	give	VERB
eurjchem-208	33	118	the	the	DET
eurjchem-208	33	119	corresponding	corresponding	ADJ
eurjchem-208	33	120	phosphonic	phosphonic	ADJ
eurjchem-208	33	121	dihydrazones	dihydrazone	NOUN
eurjchem-208	33	122	3a−d	3a−d	NUM
eurjchem-208	33	123	,	,	PUNCT
eurjchem-208	33	124	respectively	respectively	ADV
eurjchem-208	33	125	(	(	PUNCT
eurjchem-208	33	126	scheme	scheme	NOUN
eurjchem-208	33	127	1	1	NUM
eurjchem-208	33	128	)	)	PUNCT
eurjchem-208	33	129	.	.	PUNCT
eurjchem-208	34	1	2.2.2.1	2.2.2.1	X
eurjchem-208	34	2	.	.	PUNCT
eurjchem-208	34	3	n1,n5‐bis{1‐phenylethylidene}phosphonic	n1,n5‐bis{1‐phenylethylidene}phosphonic	ADJ
eurjchem-208	34	4	dihydrazide	dihydrazide	NOUN
eurjchem-208	34	5	(	(	PUNCT
eurjchem-208	34	6	3a	3a	NUM
eurjchem-208	34	7	)	)	PUNCT
eurjchem-208	34	8	yellow	yellow	ADJ
eurjchem-208	34	9	crystals	crystal	NOUN
eurjchem-208	34	10	from	from	ADP
eurjchem-208	34	11	ethanol	ethanol	NOUN
eurjchem-208	34	12	in	in	ADP
eurjchem-208	34	13	46	46	NUM
eurjchem-208	34	14	%	%	NOUN
eurjchem-208	34	15	yield	yield	NOUN
eurjchem-208	34	16	.	.	PUNCT
eurjchem-208	35	1	m.p	m.p	PROPN
eurjchem-208	35	2	.	.	PROPN
eurjchem-208	35	3	:	:	PUNCT
eurjchem-208	36	1	128−130	128−130	NUM
eurjchem-208	36	2	oc	oc	X
eurjchem-208	36	3	.	.	PROPN
eurjchem-208	36	4	ir	ir	PROPN
eurjchem-208	36	5	(	(	PUNCT
eurjchem-208	36	6	kbr	kbr	PROPN
eurjchem-208	36	7	,	,	PUNCT
eurjchem-208	36	8	max	max	PROPN
eurjchem-208	36	9	,	,	PUNCT
eurjchem-208	36	10	cm‐1	cm‐1	NUM
eurjchem-208	36	11	):	):	PUNCT
eurjchem-208	36	12	3423	3423	NUM
eurjchem-208	36	13	(	(	PUNCT
eurjchem-208	36	14	br	br	PROPN
eurjchem-208	36	15	,	,	PUNCT
eurjchem-208	36	16	nh	nh	PROPN
eurjchem-208	36	17	)	)	PUNCT
eurjchem-208	36	18	,	,	PUNCT
eurjchem-208	36	19	3053	3053	NUM
eurjchem-208	36	20	(	(	PUNCT
eurjchem-208	36	21	c−harom	c−harom	NOUN
eurjchem-208	36	22	)	)	PUNCT
eurjchem-208	36	23	,	,	PUNCT
eurjchem-208	36	24	2960	2960	NUM
eurjchem-208	36	25	(	(	PUNCT
eurjchem-208	36	26	c−haliph	c−haliph	NOUN
eurjchem-208	36	27	)	)	PUNCT
eurjchem-208	36	28	,	,	PUNCT
eurjchem-208	36	29	2339	2339	NUM
eurjchem-208	36	30	(	(	PUNCT
eurjchem-208	36	31	p−h	p−h	PROPN
eurjchem-208	36	32	)	)	PUNCT
eurjchem-208	36	33	,	,	PUNCT
eurjchem-208	36	34	1599	1599	NUM
eurjchem-208	36	35	(	(	PUNCT
eurjchem-208	36	36	c	c	NOUN
eurjchem-208	36	37	=	=	SYM
eurjchem-208	36	38	n	n	NUM
eurjchem-208	36	39	)	)	PUNCT
eurjchem-208	36	40	,	,	PUNCT
eurjchem-208	36	41	1562	1562	NUM
eurjchem-208	36	42	(	(	PUNCT
eurjchem-208	36	43	c	c	NOUN
eurjchem-208	36	44	=	=	SYM
eurjchem-208	36	45	c	c	NOUN
eurjchem-208	36	46	)	)	PUNCT
eurjchem-208	36	47	,	,	PUNCT
eurjchem-208	36	48	1284	1284	NUM
eurjchem-208	36	49	(	(	PUNCT
eurjchem-208	36	50	p	p	NOUN
eurjchem-208	36	51	=	=	NOUN
eurjchem-208	36	52	o	o	NOUN
eurjchem-208	36	53	)	)	PUNCT
eurjchem-208	36	54	.	.	PUNCT
eurjchem-208	37	1	1h	1h	NUM
eurjchem-208	37	2	nmr	nmr	NOUN
eurjchem-208	37	3	(	(	PUNCT
eurjchem-208	37	4	dmso	dmso	NOUN
eurjchem-208	37	5	,	,	PUNCT
eurjchem-208	37	6	δ	δ	PROPN
eurjchem-208	37	7	ppm	ppm	VERB
eurjchem-208	37	8	):	):	PUNCT
eurjchem-208	37	9	2.28	2.28	NUM
eurjchem-208	37	10	(	(	PUNCT
eurjchem-208	37	11	s	s	PROPN
eurjchem-208	37	12	,	,	PUNCT
eurjchem-208	37	13	6h	6h	NUM
eurjchem-208	37	14	,	,	PUNCT
eurjchem-208	37	15	ch3	ch3	PROPN
eurjchem-208	37	16	)	)	PUNCT
eurjchem-208	37	17	,	,	PUNCT
eurjchem-208	37	18	7.47−7.93	7.47−7.93	PROPN
eurjchem-208	37	19	(	(	PUNCT
eurjchem-208	37	20	m	m	PROPN
eurjchem-208	37	21	,	,	PUNCT
eurjchem-208	37	22	10h	10h	NUM
eurjchem-208	37	23	,	,	PUNCT
eurjchem-208	37	24	ph−h	ph−h	NOUN
eurjchem-208	37	25	)	)	PUNCT
eurjchem-208	37	26	.	.	PUNCT
eurjchem-208	38	1	13c	13c	NOUN
eurjchem-208	38	2	nmr	nmr	NOUN
eurjchem-208	38	3	(	(	PUNCT
eurjchem-208	38	4	dmso	dmso	NOUN
eurjchem-208	38	5	,	,	PUNCT
eurjchem-208	38	6	δ	δ	PROPN
eurjchem-208	38	7	ppm):14.7	ppm):14.7	NOUN
eurjchem-208	38	8	(	(	PUNCT
eurjchem-208	38	9	ch3	ch3	PROPN
eurjchem-208	38	10	)	)	PUNCT
eurjchem-208	38	11	,	,	PUNCT
eurjchem-208	38	12	126.4	126.4	NUM
eurjchem-208	38	13	(	(	PUNCT
eurjchem-208	38	14	c3,5),128.3	c3,5),128.3	PROPN
eurjchem-208	38	15	(	(	PUNCT
eurjchem-208	38	16	c2,6	c2,6	PROPN
eurjchem-208	38	17	)	)	PUNCT
eurjchem-208	38	18	,	,	PUNCT
eurjchem-208	38	19	129.6	129.6	NUM
eurjchem-208	38	20	(	(	PUNCT
eurjchem-208	38	21	c4	c4	NOUN
eurjchem-208	38	22	)	)	PUNCT
eurjchem-208	38	23	,	,	PUNCT
eurjchem-208	38	24	137.8	137.8	NUM
eurjchem-208	38	25	(	(	PUNCT
eurjchem-208	38	26	c1	c1	PROPN
eurjchem-208	38	27	)	)	PUNCT
eurjchem-208	38	28	,	,	PUNCT
eurjchem-208	38	29	157.2	157.2	NUM
eurjchem-208	38	30	(	(	PUNCT
eurjchem-208	38	31	c	c	NOUN
eurjchem-208	38	32	=	=	SYM
eurjchem-208	38	33	n	n	NUM
eurjchem-208	38	34	)	)	PUNCT
eurjchem-208	38	35	.	.	PUNCT
eurjchem-208	39	1	ms	ms	NOUN
eurjchem-208	39	2	(	(	PUNCT
eurjchem-208	39	3	m	m	PROPN
eurjchem-208	39	4	/	/	SYM
eurjchem-208	39	5	e	e	NOUN
eurjchem-208	39	6	,	,	PUNCT
eurjchem-208	39	7	%	%	INTJ
eurjchem-208	39	8	):	):	PUNCT
eurjchem-208	39	9	237	237	NUM
eurjchem-208	39	10	(	(	PUNCT
eurjchem-208	39	11	m+−ph	m+−ph	NOUN
eurjchem-208	39	12	,	,	PUNCT
eurjchem-208	39	13	5	5	NUM
eurjchem-208	39	14	%	%	NOUN
eurjchem-208	39	15	)	)	PUNCT
eurjchem-208	39	16	,	,	PUNCT
eurjchem-208	39	17	222	222	NUM
eurjchem-208	39	18	(	(	PUNCT
eurjchem-208	39	19	4.5	4.5	NUM
eurjchem-208	39	20	)	)	PUNCT
eurjchem-208	39	21	,	,	PUNCT
eurjchem-208	39	22	221	221	NUM
eurjchem-208	39	23	(	(	PUNCT
eurjchem-208	39	24	35	35	NUM
eurjchem-208	39	25	)	)	PUNCT
eurjchem-208	39	26	,	,	PUNCT
eurjchem-208	39	27	159	159	NUM
eurjchem-208	39	28	(	(	PUNCT
eurjchem-208	39	29	12	12	NUM
eurjchem-208	39	30	)	)	PUNCT
eurjchem-208	39	31	,	,	PUNCT
eurjchem-208	39	32	118	118	NUM
eurjchem-208	39	33	(	(	PUNCT
eurjchem-208	39	34	15	15	NUM
eurjchem-208	39	35	)	)	PUNCT
eurjchem-208	39	36	,	,	PUNCT
eurjchem-208	39	37	103	103	NUM
eurjchem-208	39	38	(	(	PUNCT
eurjchem-208	39	39	28	28	NUM
eurjchem-208	39	40	)	)	PUNCT
eurjchem-208	39	41	,	,	PUNCT
eurjchem-208	39	42	77	77	NUM
eurjchem-208	39	43	(	(	PUNCT
eurjchem-208	39	44	100	100	NUM
eurjchem-208	39	45	)	)	PUNCT
eurjchem-208	39	46	,	,	PUNCT
eurjchem-208	39	47	51	51	NUM
eurjchem-208	39	48	(	(	PUNCT
eurjchem-208	39	49	92	92	NUM
eurjchem-208	39	50	)	)	PUNCT
eurjchem-208	39	51	.	.	PUNCT
eurjchem-208	40	1	anal	anal	PROPN
eurjchem-208	40	2	.	.	PUNCT
eurjchem-208	40	3	calcd	calcd	NOUN
eurjchem-208	40	4	.	.	PUNCT
eurjchem-208	41	1	for	for	ADP
eurjchem-208	41	2	c16h19n4op	c16h19n4op	PROPN
eurjchem-208	41	3	c	c	PROPN
eurjchem-208	41	4	,	,	PUNCT
eurjchem-208	41	5	61.14	61.14	NUM
eurjchem-208	41	6	;	;	PUNCT
eurjchem-208	41	7	h	h	NOUN
eurjchem-208	41	8	,	,	PUNCT
eurjchem-208	41	9	6.09	6.09	NUM
eurjchem-208	41	10	;	;	PUNCT
eurjchem-208	41	11	n	n	CCONJ
eurjchem-208	41	12	,	,	PUNCT
eurjchem-208	41	13	17.82	17.82	NUM
eurjchem-208	41	14	.	.	PUNCT
eurjchem-208	41	15	found	find	VERB
eurjchem-208	41	16	:	:	PUNCT
eurjchem-208	42	1	c	c	X
eurjchem-208	42	2	,	,	PUNCT
eurjchem-208	42	3	60.67	60.67	NUM
eurjchem-208	42	4	;	;	PUNCT
eurjchem-208	42	5	h	h	NOUN
eurjchem-208	42	6	,	,	PUNCT
eurjchem-208	42	7	5.82	5.82	NUM
eurjchem-208	42	8	;	;	PUNCT
eurjchem-208	42	9	n	n	CCONJ
eurjchem-208	42	10	,	,	PUNCT
eurjchem-208	42	11	17.53	17.53	NUM
eurjchem-208	42	12	%	%	NOUN
eurjchem-208	42	13	.	.	PUNCT
eurjchem-208	43	1	2.2.2.2	2.2.2.2	X
eurjchem-208	43	2	.	.	PROPN
eurjchem-208	43	3	n1,n5‐bis{1‐(4`‐biphenyl)ethylidene}phosphonic	n1,n5‐bis{1‐(4`‐biphenyl)ethylidene}phosphonic	PROPN
eurjchem-208	43	4	dihydrazide	dihydrazide	PROPN
eurjchem-208	43	5	(	(	PUNCT
eurjchem-208	43	6	3b	3b	NUM
eurjchem-208	43	7	)	)	PUNCT
eurjchem-208	43	8	pale	pale	ADJ
eurjchem-208	43	9	yellow	yellow	ADJ
eurjchem-208	43	10	crystals	crystal	NOUN
eurjchem-208	43	11	from	from	ADP
eurjchem-208	43	12	dilute	dilute	NOUN
eurjchem-208	43	13	dimethylsulfoxide	dimethylsulfoxide	ADV
eurjchem-208	43	14	in	in	ADP
eurjchem-208	43	15	71	71	NUM
eurjchem-208	43	16	%	%	NOUN
eurjchem-208	43	17	yield	yield	NOUN
eurjchem-208	43	18	.	.	PUNCT
eurjchem-208	44	1	m.p	m.p	PROPN
eurjchem-208	44	2	.	.	PROPN
eurjchem-208	44	3	:	:	PUNCT
eurjchem-208	45	1	282−284	282−284	NUM
eurjchem-208	45	2	oc	oc	PROPN
eurjchem-208	45	3	.	.	PROPN
eurjchem-208	45	4	ir	ir	PROPN
eurjchem-208	45	5	(	(	PUNCT
eurjchem-208	45	6	kbr	kbr	PROPN
eurjchem-208	45	7	,	,	PUNCT
eurjchem-208	45	8	max	max	PROPN
eurjchem-208	45	9	,	,	PUNCT
eurjchem-208	45	10	cm‐1	cm‐1	PROPN
eurjchem-208	45	11	):	):	PUNCT
eurjchem-208	45	12	3425	3425	NUM
eurjchem-208	45	13	(	(	PUNCT
eurjchem-208	45	14	br	br	PROPN
eurjchem-208	45	15	,	,	PUNCT
eurjchem-208	45	16	nh	nh	PROPN
eurjchem-208	45	17	)	)	PUNCT
eurjchem-208	45	18	,	,	PUNCT
eurjchem-208	45	19	3054	3054	NUM
eurjchem-208	45	20	,	,	PUNCT
eurjchem-208	45	21	3032	3032	NUM
eurjchem-208	45	22	(	(	PUNCT
eurjchem-208	45	23	c−harom	c−harom	NOUN
eurjchem-208	45	24	)	)	PUNCT
eurjchem-208	45	25	,	,	PUNCT
eurjchem-208	45	26	2964	2964	NUM
eurjchem-208	45	27	(	(	PUNCT
eurjchem-208	45	28	c−haliph	c−haliph	NOUN
eurjchem-208	45	29	)	)	PUNCT
eurjchem-208	45	30	,	,	PUNCT
eurjchem-208	45	31	2373	2373	NUM
eurjchem-208	45	32	(	(	PUNCT
eurjchem-208	45	33	p−h	p−h	PROPN
eurjchem-208	45	34	)	)	PUNCT
eurjchem-208	45	35	,	,	PUNCT
eurjchem-208	45	36	1599	1599	NUM
eurjchem-208	45	37	(	(	PUNCT
eurjchem-208	45	38	c	c	NOUN
eurjchem-208	45	39	=	=	SYM
eurjchem-208	45	40	n	n	NUM
eurjchem-208	45	41	)	)	PUNCT
eurjchem-208	45	42	,	,	PUNCT
eurjchem-208	45	43	1577	1577	NUM
eurjchem-208	45	44	(	(	PUNCT
eurjchem-208	45	45	c	c	NOUN
eurjchem-208	45	46	=	=	SYM
eurjchem-208	45	47	c	c	NOUN
eurjchem-208	45	48	)	)	PUNCT
eurjchem-208	45	49	,	,	PUNCT
eurjchem-208	45	50	1294	1294	NUM
eurjchem-208	45	51	(	(	PUNCT
eurjchem-208	45	52	p	p	NOUN
eurjchem-208	45	53	=	=	NOUN
eurjchem-208	45	54	o	o	NOUN
eurjchem-208	45	55	)	)	PUNCT
eurjchem-208	45	56	.	.	PUNCT
eurjchem-208	46	1	1h	1h	NUM
eurjchem-208	46	2	nmr	nmr	NOUN
eurjchem-208	46	3	(	(	PUNCT
eurjchem-208	46	4	dmso	dmso	NOUN
eurjchem-208	46	5	,	,	PUNCT
eurjchem-208	46	6	δ	δ	PROPN
eurjchem-208	46	7	ppm	ppm	VERB
eurjchem-208	46	8	):	):	PUNCT
eurjchem-208	46	9	2.12	2.12	NUM
eurjchem-208	46	10	(	(	PUNCT
eurjchem-208	46	11	s	s	PROPN
eurjchem-208	46	12	,	,	PUNCT
eurjchem-208	46	13	6h	6h	NUM
eurjchem-208	46	14	,	,	PUNCT
eurjchem-208	46	15	ch3	ch3	PROPN
eurjchem-208	46	16	)	)	PUNCT
eurjchem-208	46	17	,	,	PUNCT
eurjchem-208	46	18	7.38−8.06	7.38−8.06	NUM
eurjchem-208	46	19	(	(	PUNCT
eurjchem-208	46	20	m	m	PROPN
eurjchem-208	46	21	,	,	PUNCT
eurjchem-208	46	22	18h	18h	NOUN
eurjchem-208	46	23	,	,	PUNCT
eurjchem-208	46	24	ar−h	ar−h	NOUN
eurjchem-208	46	25	)	)	PUNCT
eurjchem-208	46	26	.	.	PUNCT
eurjchem-208	47	1	ms	ms	NOUN
eurjchem-208	47	2	(	(	PUNCT
eurjchem-208	47	3	m	m	PROPN
eurjchem-208	47	4	/	/	SYM
eurjchem-208	47	5	e	e	NOUN
eurjchem-208	47	6	,	,	PUNCT
eurjchem-208	47	7	%	%	INTJ
eurjchem-208	47	8	):	):	PUNCT
eurjchem-208	47	9	389	389	NUM
eurjchem-208	47	10	(	(	PUNCT
eurjchem-208	47	11	m+−ph	m+−ph	NOUN
eurjchem-208	47	12	,	,	PUNCT
eurjchem-208	47	13	6	6	NUM
eurjchem-208	47	14	%	%	NOUN
eurjchem-208	47	15	)	)	PUNCT
eurjchem-208	47	16	,	,	PUNCT
eurjchem-208	47	17	388	388	NUM
eurjchem-208	47	18	(	(	PUNCT
eurjchem-208	47	19	31	31	NUM
eurjchem-208	47	20	)	)	PUNCT
eurjchem-208	47	21	,	,	PUNCT
eurjchem-208	47	22	373	373	NUM
eurjchem-208	47	23	(	(	PUNCT
eurjchem-208	47	24	57	57	NUM
eurjchem-208	47	25	)	)	PUNCT
eurjchem-208	47	26	,	,	PUNCT
eurjchem-208	47	27	209	209	NUM
eurjchem-208	47	28	(	(	PUNCT
eurjchem-208	47	29	12	12	NUM
eurjchem-208	47	30	)	)	PUNCT
eurjchem-208	47	31	,	,	PUNCT
eurjchem-208	47	32	194	194	NUM
eurjchem-208	47	33	(	(	PUNCT
eurjchem-208	47	34	25	25	NUM
eurjchem-208	47	35	)	)	PUNCT
eurjchem-208	47	36	,	,	PUNCT
eurjchem-208	47	37	178	178	NUM
eurjchem-208	47	38	(	(	PUNCT
eurjchem-208	47	39	31	31	NUM
eurjchem-208	47	40	)	)	PUNCT
eurjchem-208	47	41	,	,	PUNCT
eurjchem-208	47	42	153	153	NUM
eurjchem-208	47	43	(	(	PUNCT
eurjchem-208	47	44	29	29	NUM
eurjchem-208	47	45	)	)	PUNCT
eurjchem-208	47	46	,	,	PUNCT
eurjchem-208	47	47	152	152	NUM
eurjchem-208	47	48	(	(	PUNCT
eurjchem-208	47	49	100	100	NUM
eurjchem-208	47	50	)	)	PUNCT
eurjchem-208	47	51	,	,	PUNCT
eurjchem-208	47	52	76	76	NUM
eurjchem-208	47	53	(	(	PUNCT
eurjchem-208	47	54	32	32	NUM
eurjchem-208	47	55	)	)	PUNCT
eurjchem-208	47	56	,	,	PUNCT
eurjchem-208	47	57	51	51	NUM
eurjchem-208	47	58	(	(	PUNCT
eurjchem-208	47	59	19	19	NUM
eurjchem-208	47	60	)	)	PUNCT
eurjchem-208	47	61	.	.	PUNCT
eurjchem-208	48	1	anal	anal	PROPN
eurjchem-208	48	2	.	.	PUNCT
eurjchem-208	48	3	calcd	calcd	NOUN
eurjchem-208	48	4	.	.	PUNCT
eurjchem-208	49	1	for	for	ADP
eurjchem-208	49	2	c28h27n4op	c28h27n4op	NOUN
eurjchem-208	49	3	:	:	PUNCT
eurjchem-208	49	4	c	c	X
eurjchem-208	49	5	,	,	PUNCT
eurjchem-208	49	6	72.09	72.09	NUM
eurjchem-208	49	7	;	;	PUNCT
eurjchem-208	49	8	h	h	NOUN
eurjchem-208	49	9	,	,	PUNCT
eurjchem-208	49	10	5.83	5.83	NUM
eurjchem-208	49	11	;	;	PUNCT
eurjchem-208	49	12	n	n	CCONJ
eurjchem-208	49	13	,	,	PUNCT
eurjchem-208	49	14	12.01	12.01	NUM
eurjchem-208	49	15	.	.	PUNCT
eurjchem-208	49	16	found	find	VERB
eurjchem-208	49	17	:	:	PUNCT
eurjchem-208	50	1	c	c	X
eurjchem-208	50	2	,	,	PUNCT
eurjchem-208	50	3	71.72	71.72	NUM
eurjchem-208	50	4	;	;	PUNCT
eurjchem-208	50	5	h	h	NOUN
eurjchem-208	50	6	,	,	PUNCT
eurjchem-208	50	7	5.59	5.59	NUM
eurjchem-208	50	8	;	;	PUNCT
eurjchem-208	50	9	n	n	CCONJ
eurjchem-208	50	10	,	,	PUNCT
eurjchem-208	50	11	11.79	11.79	NUM
eurjchem-208	50	12	%	%	NOUN
eurjchem-208	50	13	.	.	PUNCT
eurjchem-208	51	1	2.2.2.3	2.2.2.3	X
eurjchem-208	51	2	.	.	PUNCT
eurjchem-208	52	1	n1,n5‐bis{1‐(2‐hydroxyphenyl)ethylidene	n1,n5‐bis{1‐(2‐hydroxyphenyl)ethylidene	ADJ
eurjchem-208	52	2	}	}	PUNCT
eurjchem-208	52	3	phosphonicdihydrazide	phosphonicdihydrazide	NOUN
eurjchem-208	52	4	(	(	PUNCT
eurjchem-208	52	5	3c	3c	NUM
eurjchem-208	52	6	)	)	PUNCT
eurjchem-208	52	7	yellow	yellow	ADJ
eurjchem-208	52	8	crystals	crystal	NOUN
eurjchem-208	52	9	from	from	ADP
eurjchem-208	52	10	dimethylformamide	dimethylformamide	NOUN
eurjchem-208	52	11	in	in	ADP
eurjchem-208	52	12	70	70	NUM
eurjchem-208	52	13	%	%	NOUN
eurjchem-208	52	14	yield	yield	NOUN
eurjchem-208	52	15	.	.	PUNCT
eurjchem-208	53	1	m.p	m.p	PROPN
eurjchem-208	53	2	.	.	PROPN
eurjchem-208	53	3	:	:	PUNCT
eurjchem-208	54	1	202−204oc	202−204oc	NUM
eurjchem-208	54	2	.	.	PUNCT
eurjchem-208	55	1	ir	ir	PROPN
eurjchem-208	55	2	(	(	PUNCT
eurjchem-208	55	3	kbr	kbr	PROPN
eurjchem-208	55	4	,	,	PUNCT
eurjchem-208	55	5	max	max	PROPN
eurjchem-208	55	6	,	,	PUNCT
eurjchem-208	55	7	cm‐1	cm‐1	PROPN
eurjchem-208	55	8	):	):	PUNCT
eurjchem-208	55	9	3150	3150	NUM
eurjchem-208	55	10	(	(	PUNCT
eurjchem-208	55	11	br	br	PROPN
eurjchem-208	55	12	,	,	PUNCT
eurjchem-208	55	13	oh	oh	INTJ
eurjchem-208	55	14	,	,	PUNCT
eurjchem-208	55	15	nh	nh	PROPN
eurjchem-208	55	16	)	)	PUNCT
eurjchem-208	55	17	,	,	PUNCT
eurjchem-208	55	18	3050	3050	NUM
eurjchem-208	55	19	(	(	PUNCT
eurjchem-208	55	20	c−harom	c−harom	NOUN
eurjchem-208	55	21	)	)	PUNCT
eurjchem-208	55	22	,	,	PUNCT
eurjchem-208	55	23	2924	2924	NUM
eurjchem-208	55	24	(	(	PUNCT
eurjchem-208	55	25	c−haliph	c−haliph	NOUN
eurjchem-208	55	26	)	)	PUNCT
eurjchem-208	55	27	,	,	PUNCT
eurjchem-208	55	28	2441	2441	NUM
eurjchem-208	55	29	(	(	PUNCT
eurjchem-208	55	30	br	br	PROPN
eurjchem-208	55	31	,	,	PUNCT
eurjchem-208	55	32	p−h	p−h	PROPN
eurjchem-208	55	33	)	)	PUNCT
eurjchem-208	55	34	,	,	PUNCT
eurjchem-208	55	35	1604	1604	NUM
eurjchem-208	55	36	(	(	PUNCT
eurjchem-208	55	37	c	c	NOUN
eurjchem-208	55	38	=	=	SYM
eurjchem-208	55	39	n	n	NUM
eurjchem-208	55	40	)	)	PUNCT
eurjchem-208	55	41	,	,	PUNCT
eurjchem-208	55	42	1559	1559	NUM
eurjchem-208	55	43	(	(	PUNCT
eurjchem-208	55	44	c	c	NOUN
eurjchem-208	55	45	=	=	SYM
eurjchem-208	55	46	c	c	NOUN
eurjchem-208	55	47	)	)	PUNCT
eurjchem-208	55	48	,	,	PUNCT
eurjchem-208	55	49	1245	1245	NUM
eurjchem-208	55	50	(	(	PUNCT
eurjchem-208	55	51	p	p	NOUN
eurjchem-208	55	52	=	=	NOUN
eurjchem-208	55	53	o	o	NOUN
eurjchem-208	55	54	)	)	PUNCT
eurjchem-208	55	55	.	.	PUNCT
eurjchem-208	56	1	1h	1h	NUM
eurjchem-208	56	2	nmr	nmr	NOUN
eurjchem-208	56	3	(	(	PUNCT
eurjchem-208	56	4	dmso	dmso	NOUN
eurjchem-208	56	5	,	,	PUNCT
eurjchem-208	56	6	δ	δ	PROPN
eurjchem-208	56	7	ppm	ppm	VERB
eurjchem-208	56	8	):	):	PUNCT
eurjchem-208	56	9	2.08	2.08	NUM
eurjchem-208	56	10	(	(	PUNCT
eurjchem-208	56	11	s	s	PROPN
eurjchem-208	56	12	,	,	PUNCT
eurjchem-208	56	13	6h	6h	NUM
eurjchem-208	56	14	,	,	PUNCT
eurjchem-208	56	15	ch3	ch3	PROPN
eurjchem-208	56	16	)	)	PUNCT
eurjchem-208	56	17	,	,	PUNCT
eurjchem-208	56	18	6.97	6.97	NUM
eurjchem-208	56	19	(	(	PUNCT
eurjchem-208	56	20	d	d	PROPN
eurjchem-208	56	21	,	,	PUNCT
eurjchem-208	56	22	4h	4h	NUM
eurjchem-208	56	23	,	,	PUNCT
eurjchem-208	56	24	j=8.2	j=8.2	NOUN
eurjchem-208	56	25	hz	hz	VERB
eurjchem-208	56	26	,	,	PUNCT
eurjchem-208	56	27	ar−h	ar−h	NOUN
eurjchem-208	56	28	)	)	PUNCT
eurjchem-208	56	29	,	,	PUNCT
eurjchem-208	56	30	7.40	7.40	NUM
eurjchem-208	56	31	(	(	PUNCT
eurjchem-208	56	32	t	t	PROPN
eurjchem-208	56	33	,	,	PUNCT
eurjchem-208	56	34	2h	2h	NUM
eurjchem-208	56	35	,	,	PUNCT
eurjchem-208	56	36	j=7.4	j=7.4	PROPN
eurjchem-208	56	37	hz	hz	VERB
eurjchem-208	56	38	,	,	PUNCT
eurjchem-208	56	39	ar−h	ar−h	NOUN
eurjchem-208	56	40	)	)	PUNCT
eurjchem-208	56	41	,	,	PUNCT
eurjchem-208	56	42	7.76	7.76	NUM
eurjchem-208	56	43	(	(	PUNCT
eurjchem-208	56	44	d	d	PROPN
eurjchem-208	56	45	,	,	PUNCT
eurjchem-208	56	46	2h	2h	NUM
eurjchem-208	56	47	,	,	PUNCT
eurjchem-208	56	48	j=7.6	j=7.6	NOUN
eurjchem-208	56	49	hz	hz	VERB
eurjchem-208	56	50	,	,	PUNCT
eurjchem-208	56	51	ar−h	ar−h	NOUN
eurjchem-208	56	52	)	)	PUNCT
eurjchem-208	56	53	,	,	PUNCT
eurjchem-208	56	54	12.90	12.90	NUM
eurjchem-208	56	55	(	(	PUNCT
eurjchem-208	56	56	s	s	PROPN
eurjchem-208	56	57	,	,	PUNCT
eurjchem-208	56	58	2h	2h	NUM
eurjchem-208	56	59	,	,	PUNCT
eurjchem-208	56	60	oh	oh	INTJ
eurjchem-208	56	61	exchangeable	exchangeable	ADJ
eurjchem-208	56	62	with	with	ADP
eurjchem-208	56	63	d2o).31p	d2o).31p	NOUN
eurjchem-208	56	64	nmr	nmr	NOUN
eurjchem-208	56	65	(	(	PUNCT
eurjchem-208	56	66	dmso	dmso	NOUN
eurjchem-208	56	67	,	,	PUNCT
eurjchem-208	56	68	δ	δ	PROPN
eurjchem-208	56	69	ppm	ppm	VERB
eurjchem-208	56	70	):	):	PUNCT
eurjchem-208	56	71	18.4	18.4	NUM
eurjchem-208	56	72	.	.	PUNCT
eurjchem-208	57	1	ms	ms	NOUN
eurjchem-208	57	2	(	(	PUNCT
eurjchem-208	57	3	m	m	PROPN
eurjchem-208	57	4	/	/	SYM
eurjchem-208	57	5	e	e	NOUN
eurjchem-208	57	6	,	,	PUNCT
eurjchem-208	57	7	%	%	INTJ
eurjchem-208	57	8	):	):	PUNCT
eurjchem-208	57	9	348	348	NUM
eurjchem-208	57	10	(	(	PUNCT
eurjchem-208	57	11	m+2	m+2	NOUN
eurjchem-208	57	12	,	,	PUNCT
eurjchem-208	57	13	12	12	NUM
eurjchem-208	57	14	%	%	NOUN
eurjchem-208	57	15	)	)	PUNCT
eurjchem-208	57	16	,	,	PUNCT
eurjchem-208	57	17	302	302	NUM
eurjchem-208	57	18	(	(	PUNCT
eurjchem-208	57	19	9	9	NUM
eurjchem-208	57	20	)	)	PUNCT
eurjchem-208	57	21	,	,	PUNCT
eurjchem-208	57	22	301	301	NUM
eurjchem-208	57	23	(	(	PUNCT
eurjchem-208	57	24	12	12	NUM
eurjchem-208	57	25	)	)	PUNCT
eurjchem-208	57	26	,	,	PUNCT
eurjchem-208	57	27	119	119	NUM
eurjchem-208	57	28	(	(	PUNCT
eurjchem-208	57	29	14	14	NUM
eurjchem-208	57	30	)	)	PUNCT
eurjchem-208	57	31	,	,	PUNCT
eurjchem-208	57	32	80	80	NUM
eurjchem-208	57	33	(	(	PUNCT
eurjchem-208	57	34	44	44	NUM
eurjchem-208	57	35	)	)	PUNCT
eurjchem-208	57	36	,	,	PUNCT
eurjchem-208	57	37	77	77	NUM
eurjchem-208	57	38	(	(	PUNCT
eurjchem-208	57	39	14	14	NUM
eurjchem-208	57	40	)	)	PUNCT
eurjchem-208	57	41	,	,	PUNCT
eurjchem-208	57	42	64	64	NUM
eurjchem-208	57	43	(	(	PUNCT
eurjchem-208	57	44	100	100	NUM
eurjchem-208	57	45	)	)	PUNCT
eurjchem-208	57	46	,	,	PUNCT
eurjchem-208	57	47	52	52	NUM
eurjchem-208	57	48	(	(	PUNCT
eurjchem-208	57	49	42	42	NUM
eurjchem-208	57	50	)	)	PUNCT
eurjchem-208	57	51	.	.	PUNCT
eurjchem-208	58	1	anal	anal	PROPN
eurjchem-208	58	2	.	.	PUNCT
eurjchem-208	58	3	calcd	calcd	NOUN
eurjchem-208	58	4	.	.	PUNCT
eurjchem-208	59	1	for	for	ADP
eurjchem-208	59	2	c16h19n4o3p	c16h19n4o3p	PROPN
eurjchem-208	59	3	:	:	PUNCT
eurjchem-208	59	4	c	c	X
eurjchem-208	59	5	,	,	PUNCT
eurjchem-208	59	6	55.49	55.49	NUM
eurjchem-208	59	7	;	;	PUNCT
eurjchem-208	59	8	h	h	NOUN
eurjchem-208	59	9	,	,	PUNCT
eurjchem-208	59	10	5.53	5.53	NUM
eurjchem-208	59	11	;	;	PUNCT
eurjchem-208	59	12	n	n	CCONJ
eurjchem-208	59	13	,	,	PUNCT
eurjchem-208	59	14	16.18	16.18	NUM
eurjchem-208	59	15	.	.	PUNCT
eurjchem-208	59	16	found	find	VERB
eurjchem-208	59	17	:	:	PUNCT
eurjchem-208	60	1	c	c	X
eurjchem-208	60	2	,	,	PUNCT
eurjchem-208	60	3	55.14	55.14	NUM
eurjchem-208	60	4	;	;	PUNCT
eurjchem-208	60	5	h	h	NOUN
eurjchem-208	60	6	,	,	PUNCT
eurjchem-208	60	7	5.24	5.24	NUM
eurjchem-208	60	8	;	;	PUNCT
eurjchem-208	60	9	n	n	CCONJ
eurjchem-208	60	10	,	,	PUNCT
eurjchem-208	60	11	15.68	15.68	NUM
eurjchem-208	60	12	%	%	NOUN
eurjchem-208	60	13	.	.	PUNCT
eurjchem-208	61	1	2.2.2.4	2.2.2.4	X
eurjchem-208	61	2	.	.	X
eurjchem-208	61	3	n1,n5‐bis{1‐(2‐methyl‐4‐oxo‐4h‐chromen‐3‐	n1,n5‐bis{1‐(2‐methyl‐4‐oxo‐4h‐chromen‐3‐	PROPN
eurjchem-208	61	4	yl)ethylidene}phosphonic	yl)ethylidene}phosphonic	NUM
eurjchem-208	61	5	dihydrazide	dihydrazide	NOUN
eurjchem-208	61	6	(	(	PUNCT
eurjchem-208	61	7	3d	3d	NOUN
eurjchem-208	61	8	)	)	PUNCT
eurjchem-208	61	9	pale	pale	ADJ
eurjchem-208	61	10	yellow	yellow	ADJ
eurjchem-208	61	11	crystals	crystal	NOUN
eurjchem-208	61	12	from	from	ADP
eurjchem-208	61	13	dimethylformamide	dimethylformamide	NOUN
eurjchem-208	61	14	in	in	ADP
eurjchem-208	61	15	69	69	NUM
eurjchem-208	61	16	%	%	NOUN
eurjchem-208	61	17	yield	yield	NOUN
eurjchem-208	61	18	.	.	PUNCT
eurjchem-208	62	1	m.p	m.p	PROPN
eurjchem-208	62	2	.	.	PROPN
eurjchem-208	62	3	:	:	PUNCT
eurjchem-208	63	1	266−268	266−268	NUM
eurjchem-208	63	2	oc	oc	VERB
eurjchem-208	63	3	.	.	PROPN
eurjchem-208	63	4	ir	ir	PROPN
eurjchem-208	63	5	(	(	PUNCT
eurjchem-208	63	6	kbr	kbr	PROPN
eurjchem-208	63	7	,	,	PUNCT
eurjchem-208	63	8	max	max	PROPN
eurjchem-208	63	9	,	,	PUNCT
eurjchem-208	63	10	cm‐1	cm‐1	NUM
eurjchem-208	63	11	):	):	PUNCT
eurjchem-208	63	12	3241	3241	NUM
eurjchem-208	63	13	(	(	PUNCT
eurjchem-208	63	14	nh	nh	NOUN
eurjchem-208	63	15	)	)	PUNCT
eurjchem-208	63	16	,	,	PUNCT
eurjchem-208	63	17	3023	3023	NUM
eurjchem-208	63	18	(	(	PUNCT
eurjchem-208	63	19	c−harom	c−harom	NOUN
eurjchem-208	63	20	)	)	PUNCT
eurjchem-208	63	21	,	,	PUNCT
eurjchem-208	63	22	2920	2920	NUM
eurjchem-208	63	23	(	(	PUNCT
eurjchem-208	63	24	c−haliph	c−haliph	NOUN
eurjchem-208	63	25	)	)	PUNCT
eurjchem-208	63	26	,	,	PUNCT
eurjchem-208	63	27	2599	2599	NUM
eurjchem-208	63	28	(	(	PUNCT
eurjchem-208	63	29	p−h	p−h	PROPN
eurjchem-208	63	30	)	)	PUNCT
eurjchem-208	63	31	,	,	PUNCT
eurjchem-208	63	32	1665	1665	NUM
eurjchem-208	63	33	(	(	PUNCT
eurjchem-208	63	34	c	c	NOUN
eurjchem-208	63	35	=	=	NOUN
eurjchem-208	63	36	o	o	NOUN
eurjchem-208	63	37	)	)	PUNCT
eurjchem-208	63	38	,	,	PUNCT
eurjchem-208	63	39	1609	1609	NUM
eurjchem-208	63	40	(	(	PUNCT
eurjchem-208	63	41	c	c	NOUN
eurjchem-208	63	42	=	=	SYM
eurjchem-208	63	43	n	n	NUM
eurjchem-208	63	44	)	)	PUNCT
eurjchem-208	63	45	,	,	PUNCT
eurjchem-208	63	46	1528	1528	NUM
eurjchem-208	63	47	(	(	PUNCT
eurjchem-208	63	48	c	c	NOUN
eurjchem-208	63	49	=	=	SYM
eurjchem-208	63	50	c	c	NOUN
eurjchem-208	63	51	)	)	PUNCT
eurjchem-208	63	52	,	,	PUNCT
eurjchem-208	63	53	1256	1256	NUM
eurjchem-208	63	54	(	(	PUNCT
eurjchem-208	63	55	p	p	NOUN
eurjchem-208	63	56	=	=	NOUN
eurjchem-208	63	57	o	o	NOUN
eurjchem-208	63	58	)	)	PUNCT
eurjchem-208	63	59	,	,	PUNCT
eurjchem-208	63	60	1011	1011	NUM
eurjchem-208	63	61	(	(	PUNCT
eurjchem-208	63	62	c−o−c	c−o−c	NOUN
eurjchem-208	63	63	)	)	PUNCT
eurjchem-208	63	64	.	.	PUNCT
eurjchem-208	64	1	1h	1h	NUM
eurjchem-208	64	2	nmr	nmr	NOUN
eurjchem-208	64	3	(	(	PUNCT
eurjchem-208	64	4	dmso	dmso	NOUN
eurjchem-208	64	5	,	,	PUNCT
eurjchem-208	64	6	δ	δ	PROPN
eurjchem-208	64	7	ppm	ppm	VERB
eurjchem-208	64	8	):	):	PUNCT
eurjchem-208	64	9	2.07	2.07	NUM
eurjchem-208	64	10	(	(	PUNCT
eurjchem-208	64	11	s	s	PROPN
eurjchem-208	64	12	,	,	PUNCT
eurjchem-208	64	13	6h	6h	NUM
eurjchem-208	64	14	,	,	PUNCT
eurjchem-208	64	15	ch3	ch3	PROPN
eurjchem-208	64	16	)	)	PUNCT
eurjchem-208	64	17	,	,	PUNCT
eurjchem-208	64	18	2.34	2.34	NUM
eurjchem-208	64	19	(	(	PUNCT
eurjchem-208	64	20	s	s	PROPN
eurjchem-208	64	21	,	,	PUNCT
eurjchem-208	64	22	6h	6h	NUM
eurjchem-208	64	23	,	,	PUNCT
eurjchem-208	64	24	ch3	ch3	PROPN
eurjchem-208	64	25	)	)	PUNCT
eurjchem-208	64	26	,	,	PUNCT
eurjchem-208	64	27	6.88−7.74	6.88−7.74	NUM
eurjchem-208	64	28	(	(	PUNCT
eurjchem-208	64	29	m	m	PROPN
eurjchem-208	64	30	,	,	PUNCT
eurjchem-208	64	31	8h	8h	NUM
eurjchem-208	64	32	,	,	PUNCT
eurjchem-208	64	33	ar−h	ar−h	NOUN
eurjchem-208	64	34	)	)	PUNCT
eurjchem-208	64	35	.	.	PUNCT
eurjchem-208	65	1	ms	ms	NOUN
eurjchem-208	65	2	(	(	PUNCT
eurjchem-208	65	3	m	m	PROPN
eurjchem-208	65	4	/	/	SYM
eurjchem-208	65	5	e	e	NOUN
eurjchem-208	65	6	,	,	PUNCT
eurjchem-208	65	7	%	%	INTJ
eurjchem-208	65	8	):	):	PUNCT
eurjchem-208	65	9	515	515	NUM
eurjchem-208	65	10	(	(	PUNCT
eurjchem-208	65	11	m+2h2o	m+2h2o	NOUN
eurjchem-208	65	12	,	,	PUNCT
eurjchem-208	65	13	18	18	NUM
eurjchem-208	65	14	%	%	NOUN
eurjchem-208	65	15	)	)	PUNCT
eurjchem-208	65	16	,	,	PUNCT
eurjchem-208	65	17	286	286	NUM
eurjchem-208	65	18	(	(	PUNCT
eurjchem-208	65	19	30	30	NUM
eurjchem-208	65	20	)	)	PUNCT
eurjchem-208	65	21	,	,	PUNCT
eurjchem-208	65	22	200	200	NUM
eurjchem-208	65	23	(	(	PUNCT
eurjchem-208	65	24	30	30	NUM
eurjchem-208	65	25	)	)	PUNCT
eurjchem-208	65	26	,	,	PUNCT
eurjchem-208	65	27	99	99	NUM
eurjchem-208	65	28	(	(	PUNCT
eurjchem-208	65	29	30	30	NUM
eurjchem-208	65	30	)	)	PUNCT
eurjchem-208	65	31	,	,	PUNCT
eurjchem-208	65	32	77	77	NUM
eurjchem-208	65	33	(	(	PUNCT
eurjchem-208	65	34	70	70	NUM
eurjchem-208	65	35	)	)	PUNCT
eurjchem-208	65	36	,	,	PUNCT
eurjchem-208	65	37	55	55	NUM
eurjchem-208	65	38	(	(	PUNCT
eurjchem-208	65	39	100	100	NUM
eurjchem-208	65	40	)	)	PUNCT
eurjchem-208	65	41	,	,	PUNCT
eurjchem-208	65	42	51	51	NUM
eurjchem-208	65	43	(	(	PUNCT
eurjchem-208	65	44	26	26	NUM
eurjchem-208	65	45	)	)	PUNCT
eurjchem-208	65	46	.	.	PUNCT
eurjchem-208	66	1	anal	anal	PROPN
eurjchem-208	66	2	.	.	PUNCT
eurjchem-208	66	3	calcd	calcd	NOUN
eurjchem-208	66	4	.	.	PUNCT
eurjchem-208	67	1	for	for	ADP
eurjchem-208	67	2	c24h23n4o5p	c24h23n4o5p	NUM
eurjchem-208	67	3	:	:	PUNCT
eurjchem-208	67	4	c	c	X
eurjchem-208	67	5	,	,	PUNCT
eurjchem-208	67	6	60.25	60.25	NUM
eurjchem-208	67	7	;	;	PUNCT
eurjchem-208	67	8	h	h	NOUN
eurjchem-208	67	9	,	,	PUNCT
eurjchem-208	67	10	4.85	4.85	NUM
eurjchem-208	67	11	;	;	PUNCT
eurjchem-208	67	12	n	n	CCONJ
eurjchem-208	67	13	,	,	PUNCT
eurjchem-208	67	14	11.71	11.71	NUM
eurjchem-208	67	15	.	.	PUNCT
eurjchem-208	67	16	found	find	VERB
eurjchem-208	67	17	:	:	PUNCT
eurjchem-208	68	1	c	c	X
eurjchem-208	68	2	,	,	PUNCT
eurjchem-208	68	3	59.81	59.81	NUM
eurjchem-208	68	4	;	;	PUNCT
eurjchem-208	69	1	h	h	NOUN
eurjchem-208	69	2	,	,	PUNCT
eurjchem-208	69	3	4.51	4.51	NUM
eurjchem-208	69	4	;	;	PUNCT
eurjchem-208	69	5	n	n	CCONJ
eurjchem-208	69	6	,	,	PUNCT
eurjchem-208	69	7	11.29	11.29	NUM
eurjchem-208	69	8	%	%	NOUN
eurjchem-208	69	9	.	.	PUNCT
eurjchem-208	70	1	2.2.3	2.2.3	X
eurjchem-208	70	2	.	.	X
eurjchem-208	71	1	synthesis	synthesis	NOUN
eurjchem-208	71	2	of	of	ADP
eurjchem-208	71	3	compounds	compound	NOUN
eurjchem-208	71	4	4a	4a	NUM
eurjchem-208	71	5	,	,	PUNCT
eurjchem-208	71	6	4b	4b	X
eurjchem-208	71	7	,	,	PUNCT
eurjchem-208	71	8	6	6	NUM
eurjchem-208	71	9	and	and	CCONJ
eurjchem-208	71	10	8	8	NUM
eurjchem-208	71	11	:	:	PUNCT
eurjchem-208	71	12	general	general	ADJ
eurjchem-208	71	13	procedure	procedure	NOUN
eurjchem-208	71	14	for	for	ADP
eurjchem-208	71	15	vilsmeier‐haack	vilsmeier‐haack	NOUN
eurjchem-208	71	16	reaction	reaction	NOUN
eurjchem-208	71	17	of	of	ADP
eurjchem-208	71	18	phosphonic‐	phosphonic‐	PROPN
eurjchem-208	71	19	dihydrazones	dihydrazone	NOUN
eurjchem-208	71	20	(	(	PUNCT
eurjchem-208	71	21	3a‐d	3a‐d	ADV
eurjchem-208	71	22	)	)	PUNCT
eurjchem-208	71	23	the	the	DET
eurjchem-208	71	24	vilsmeier	vilsmeier	ADJ
eurjchem-208	71	25	reagent	reagent	NOUN
eurjchem-208	71	26	was	be	AUX
eurjchem-208	71	27	prepared	prepare	VERB
eurjchem-208	71	28	by	by	ADP
eurjchem-208	71	29	adding	add	VERB
eurjchem-208	71	30	dimethylformamide	dimethylformamide	NOUN
eurjchem-208	71	31	(	(	PUNCT
eurjchem-208	71	32	0.05	0.05	NUM
eurjchem-208	71	33	mol	mol	NOUN
eurjchem-208	71	34	,	,	PUNCT
eurjchem-208	71	35	3.88	3.88	NUM
eurjchem-208	71	36	cm3	cm3	NOUN
eurjchem-208	71	37	)	)	PUNCT
eurjchem-208	71	38	in	in	ADP
eurjchem-208	71	39	an	an	DET
eurjchem-208	71	40	ice‐cold	ice‐cold	VERB
eurjchem-208	71	41	condition	condition	NOUN
eurjchem-208	71	42	(	(	PUNCT
eurjchem-208	71	43	0‐5	0‐5	NOUN
eurjchem-208	71	44	oc	oc	VERB
eurjchem-208	71	45	)	)	PUNCT
eurjchem-208	71	46	under	under	ADP
eurjchem-208	71	47	constant	constant	ADJ
eurjchem-208	71	48	stirring	stirring	NOUN
eurjchem-208	71	49	.	.	PUNCT
eurjchem-208	72	1	to	to	ADP
eurjchem-208	72	2	this	this	PRON
eurjchem-208	72	3	,	,	PUNCT
eurjchem-208	72	4	phosphorus	phosphorus	NOUN
eurjchem-208	72	5	oxychloride	oxychloride	NOUN
eurjchem-208	72	6	(	(	PUNCT
eurjchem-208	72	7	0.025	0.025	NUM
eurjchem-208	72	8	mol	mol	NOUN
eurjchem-208	72	9	,	,	PUNCT
eurjchem-208	72	10	2.34	2.34	NUM
eurjchem-208	72	11	cm3	cm3	NOUN
eurjchem-208	72	12	)	)	PUNCT
eurjchem-208	72	13	was	be	AUX
eurjchem-208	72	14	added	add	VERB
eurjchem-208	72	15	dropwise	dropwise	NOUN
eurjchem-208	72	16	over	over	ADP
eurjchem-208	72	17	a	a	DET
eurjchem-208	72	18	period	period	NOUN
eurjchem-208	72	19	of	of	ADP
eurjchem-208	72	20	half	half	NOUN
eurjchem-208	72	21	hour	hour	NOUN
eurjchem-208	72	22	and	and	CCONJ
eurjchem-208	72	23	the	the	DET
eurjchem-208	72	24	resulting	result	VERB
eurjchem-208	72	25	mixture	mixture	NOUN
eurjchem-208	72	26	was	be	AUX
eurjchem-208	72	27	stirred	stir	VERB
eurjchem-208	72	28	for	for	ADP
eurjchem-208	72	29	a	a	DET
eurjchem-208	72	30	further	further	ADJ
eurjchem-208	72	31	half	half	ADJ
eurjchem-208	72	32	hour	hour	NOUN
eurjchem-208	72	33	.	.	PUNCT
eurjchem-208	73	1	each	each	DET
eurjchem-208	73	2	one	one	NUM
eurjchem-208	73	3	of	of	ADP
eurjchem-208	73	4	phosphonicdihydrazones	phosphonicdihydrazone	NOUN
eurjchem-208	73	5	3a‐d	3a‐d	ADV
eurjchem-208	73	6	(	(	PUNCT
eurjchem-208	73	7	0.005	0.005	NUM
eurjchem-208	73	8	mol	mol	NOUN
eurjchem-208	73	9	)	)	PUNCT
eurjchem-208	73	10	was	be	AUX
eurjchem-208	73	11	added	add	VERB
eurjchem-208	73	12	to	to	ADP
eurjchem-208	73	13	the	the	DET
eurjchem-208	73	14	vilsmeier	vilsmeier	NOUN
eurjchem-208	73	15	reagent	reagent	NOUN
eurjchem-208	73	16	and	and	CCONJ
eurjchem-208	73	17	stirred	stir	VERB
eurjchem-208	73	18	for	for	ADP
eurjchem-208	73	19	5	5	NUM
eurjchem-208	73	20	hours	hour	NOUN
eurjchem-208	73	21	at	at	ADP
eurjchem-208	73	22	50‐60	50‐60	NUM
eurjchem-208	73	23	oc	oc	NOUN
eurjchem-208	73	24	.	.	PUNCT
eurjchem-208	74	1	the	the	DET
eurjchem-208	74	2	reaction	reaction	NOUN
eurjchem-208	74	3	mixture	mixture	NOUN
eurjchem-208	74	4	was	be	AUX
eurjchem-208	74	5	cooled	cool	VERB
eurjchem-208	74	6	and	and	CCONJ
eurjchem-208	74	7	poured	pour	VERB
eurjchem-208	74	8	into	into	ADP
eurjchem-208	74	9	crushed	crushed	ADJ
eurjchem-208	74	10	ice	ice	NOUN
eurjchem-208	74	11	and	and	CCONJ
eurjchem-208	74	12	2	2	NUM
eurjchem-208	74	13	g	g	NOUN
eurjchem-208	74	14	of	of	ADP
eurjchem-208	74	15	sodium	sodium	NOUN
eurjchem-208	74	16	acetate	acetate	NOUN
eurjchem-208	74	17	was	be	AUX
eurjchem-208	74	18	added	add	VERB
eurjchem-208	74	19	under	under	ADP
eurjchem-208	74	20	constant	constant	ADJ
eurjchem-208	74	21	manual	manual	ADJ
eurjchem-208	74	22	stirring	stirring	NOUN
eurjchem-208	74	23	.	.	PUNCT
eurjchem-208	75	1	the	the	DET
eurjchem-208	75	2	reaction	reaction	NOUN
eurjchem-208	75	3	mixture	mixture	NOUN
eurjchem-208	75	4	was	be	AUX
eurjchem-208	75	5	kept	keep	VERB
eurjchem-208	75	6	a	a	DET
eurjchem-208	75	7	side	side	NOUN
eurjchem-208	75	8	overnight	overnight	ADV
eurjchem-208	75	9	.	.	PUNCT
eurjchem-208	76	1	the	the	DET
eurjchem-208	76	2	resulting	result	VERB
eurjchem-208	76	3	precipitate	precipitate	NOUN
eurjchem-208	76	4	was	be	AUX
eurjchem-208	76	5	filtered	filter	VERB
eurjchem-208	76	6	off	off	ADP
eurjchem-208	76	7	,	,	PUNCT
eurjchem-208	76	8	washed	wash	VERB
eurjchem-208	76	9	with	with	ADP
eurjchem-208	76	10	water	water	NOUN
eurjchem-208	76	11	several	several	ADJ
eurjchem-208	76	12	times	time	NOUN
eurjchem-208	76	13	and	and	CCONJ
eurjchem-208	76	14	crystallized	crystallize	VERB
eurjchem-208	76	15	from	from	ADP
eurjchem-208	76	16	the	the	DET
eurjchem-208	76	17	proper	proper	ADJ
eurjchem-208	76	18	solvent	solvent	NOUN
eurjchem-208	76	19	to	to	PART
eurjchem-208	76	20	give	give	VERB
eurjchem-208	76	21	the	the	DET
eurjchem-208	76	22	corresponding	correspond	VERB
eurjchem-208	76	23	products	product	NOUN
eurjchem-208	76	24	4a	4a	NOUN
eurjchem-208	76	25	,	,	PUNCT
eurjchem-208	76	26	4b	4b	X
eurjchem-208	76	27	,	,	PUNCT
eurjchem-208	76	28	6	6	NUM
eurjchem-208	76	29	and	and	CCONJ
eurjchem-208	76	30	8	8	NUM
eurjchem-208	76	31	,	,	PUNCT
eurjchem-208	76	32	respectively	respectively	ADV
eurjchem-208	76	33	.	.	PUNCT
eurjchem-208	77	1	2.2.3.1	2.2.3.1	X
eurjchem-208	77	2	.	.	PUNCT
eurjchem-208	77	3	bis{4‐formyl‐3‐phenyl‐1h‐pyrazol‐1‐yl}phosphine	bis{4‐formyl‐3‐phenyl‐1h‐pyrazol‐1‐yl}phosphine	NOUN
eurjchem-208	77	4	oxide	oxide	NOUN
eurjchem-208	77	5	(	(	PUNCT
eurjchem-208	77	6	4a	4a	NUM
eurjchem-208	77	7	)	)	PUNCT
eurjchem-208	77	8	beige	beige	ADJ
eurjchem-208	77	9	crystals	crystal	NOUN
eurjchem-208	77	10	from	from	ADP
eurjchem-208	77	11	ethanol	ethanol	NOUN
eurjchem-208	77	12	in	in	ADP
eurjchem-208	77	13	61	61	NUM
eurjchem-208	77	14	%	%	NOUN
eurjchem-208	77	15	yield	yield	NOUN
eurjchem-208	77	16	.	.	PUNCT
eurjchem-208	78	1	m.p	m.p	PROPN
eurjchem-208	78	2	.	.	PROPN
eurjchem-208	78	3	:	:	PUNCT
eurjchem-208	79	1	193−195	193−195	X
eurjchem-208	79	2	oc	oc	X
eurjchem-208	79	3	.	.	PROPN
eurjchem-208	79	4	ir	ir	PROPN
eurjchem-208	79	5	(	(	PUNCT
eurjchem-208	79	6	kbr	kbr	PROPN
eurjchem-208	79	7	,	,	PUNCT
eurjchem-208	79	8	max	max	PROPN
eurjchem-208	79	9	,	,	PUNCT
eurjchem-208	79	10	cm‐1	cm‐1	PROPN
eurjchem-208	79	11	):	):	PUNCT
eurjchem-208	79	12	3014	3014	NUM
eurjchem-208	79	13	(	(	PUNCT
eurjchem-208	79	14	c−harom	c−harom	NOUN
eurjchem-208	79	15	)	)	PUNCT
eurjchem-208	79	16	,	,	PUNCT
eurjchem-208	79	17	2771	2771	NUM
eurjchem-208	79	18	(	(	PUNCT
eurjchem-208	79	19	p−h	p−h	PROPN
eurjchem-208	79	20	)	)	PUNCT
eurjchem-208	79	21	,	,	PUNCT
eurjchem-208	79	22	1678	1678	NUM
eurjchem-208	79	23	(	(	PUNCT
eurjchem-208	79	24	c	c	NOUN
eurjchem-208	79	25	=	=	NOUN
eurjchem-208	79	26	o	o	NOUN
eurjchem-208	79	27	)	)	PUNCT
eurjchem-208	79	28	,	,	PUNCT
eurjchem-208	79	29	1620	1620	NUM
eurjchem-208	79	30	(	(	PUNCT
eurjchem-208	79	31	c	c	NOUN
eurjchem-208	79	32	=	=	SYM
eurjchem-208	79	33	n	n	NUM
eurjchem-208	79	34	)	)	PUNCT
eurjchem-208	79	35	,	,	PUNCT
eurjchem-208	79	36	1535	1535	NUM
eurjchem-208	79	37	(	(	PUNCT
eurjchem-208	79	38	c	c	NOUN
eurjchem-208	79	39	=	=	SYM
eurjchem-208	79	40	c	c	NOUN
eurjchem-208	79	41	)	)	PUNCT
eurjchem-208	79	42	,	,	PUNCT
eurjchem-208	79	43	1284	1284	NUM
eurjchem-208	79	44	(	(	PUNCT
eurjchem-208	79	45	p	p	NOUN
eurjchem-208	79	46	=	=	NOUN
eurjchem-208	79	47	o	o	NOUN
eurjchem-208	79	48	)	)	PUNCT
eurjchem-208	79	49	.	.	PUNCT
eurjchem-208	80	1	1h	1h	NUM
eurjchem-208	80	2	nmr	nmr	NOUN
eurjchem-208	80	3	(	(	PUNCT
eurjchem-208	80	4	dmso	dmso	NOUN
eurjchem-208	80	5	,	,	PUNCT
eurjchem-208	80	6	δ	δ	PROPN
eurjchem-208	80	7	ppm	ppm	VERB
eurjchem-208	80	8	):	):	PUNCT
eurjchem-208	80	9	7.45	7.45	NUM
eurjchem-208	80	10	(	(	PUNCT
eurjchem-208	80	11	d	d	PROPN
eurjchem-208	80	12	,	,	PUNCT
eurjchem-208	80	13	1h	1h	NUM
eurjchem-208	80	14	,	,	PUNCT
eurjchem-208	80	15	jph=682	jph=682	PROPN
eurjchem-208	80	16	hz	hz	NOUN
eurjchem-208	80	17	,	,	PUNCT
eurjchem-208	80	18	p−h	p−h	NOUN
eurjchem-208	80	19	)	)	PUNCT
eurjchem-208	80	20	,	,	PUNCT
eurjchem-208	80	21	7.45–7.93	7.45–7.93	NUM
eurjchem-208	80	22	(	(	PUNCT
eurjchem-208	80	23	m	m	PROPN
eurjchem-208	80	24	,	,	PUNCT
eurjchem-208	80	25	10h	10h	NUM
eurjchem-208	80	26	,	,	PUNCT
eurjchem-208	80	27	ph−h	ph−h	NOUN
eurjchem-208	80	28	)	)	PUNCT
eurjchem-208	80	29	,	,	PUNCT
eurjchem-208	80	30	8.69	8.69	NUM
eurjchem-208	80	31	(	(	PUNCT
eurjchem-208	80	32	s	s	PROPN
eurjchem-208	80	33	,	,	PUNCT
eurjchem-208	80	34	2h	2h	NUM
eurjchem-208	80	35	,	,	PUNCT
eurjchem-208	80	36	c5−hpyrazole	c5−hpyrazole	NOUN
eurjchem-208	80	37	)	)	PUNCT
eurjchem-208	80	38	,	,	PUNCT
eurjchem-208	80	39	9.95	9.95	NUM
eurjchem-208	80	40	(	(	PUNCT
eurjchem-208	80	41	s	s	PROPN
eurjchem-208	80	42	,	,	PUNCT
eurjchem-208	80	43	2h	2h	NUM
eurjchem-208	80	44	,	,	PUNCT
eurjchem-208	80	45	cho	cho	NOUN
eurjchem-208	80	46	)	)	PUNCT
eurjchem-208	80	47	.	.	PUNCT
eurjchem-208	81	1	13c	13c	NOUN
eurjchem-208	81	2	nmr	nmr	NOUN
eurjchem-208	81	3	(	(	PUNCT
eurjchem-208	81	4	dmso	dmso	NOUN
eurjchem-208	81	5	,	,	PUNCT
eurjchem-208	81	6	δ	δ	PROPN
eurjchem-208	81	7	ppm	ppm	VERB
eurjchem-208	81	8	):	):	PUNCT
eurjchem-208	81	9	121.1	121.1	NUM
eurjchem-208	81	10	(	(	PUNCT
eurjchem-208	81	11	c4pyrazole	c4pyrazole	NOUN
eurjchem-208	81	12	)	)	PUNCT
eurjchem-208	81	13	,	,	PUNCT
eurjchem-208	81	14	127.5–138.2	127.5–138.2	NUM
eurjchem-208	81	15	(	(	PUNCT
eurjchem-208	81	16	phenyl	phenyl	NOUN
eurjchem-208	81	17	carbons	carbon	NOUN
eurjchem-208	81	18	)	)	PUNCT
eurjchem-208	81	19	,	,	PUNCT
eurjchem-208	81	20	144.5	144.5	NUM
eurjchem-208	81	21	(	(	PUNCT
eurjchem-208	81	22	c5pyrazole	c5pyrazole	NOUN
eurjchem-208	81	23	)	)	PUNCT
eurjchem-208	81	24	,	,	PUNCT
eurjchem-208	81	25	152.1	152.1	NUM
eurjchem-208	81	26	(	(	PUNCT
eurjchem-208	81	27	c3pyrazole	c3pyrazole	PROPN
eurjchem-208	81	28	)	)	PUNCT
eurjchem-208	81	29	,	,	PUNCT
eurjchem-208	81	30	184.6	184.6	NUM
eurjchem-208	81	31	(	(	PUNCT
eurjchem-208	81	32	cho).ms	cho).ms	NOUN
eurjchem-208	81	33	(	(	PUNCT
eurjchem-208	81	34	m	m	NOUN
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eurjchem-208	81	36	e	e	NOUN
eurjchem-208	81	37	,	,	PUNCT
eurjchem-208	81	38	%	%	INTJ
eurjchem-208	81	39	):	):	PUNCT
eurjchem-208	81	40	389	389	NUM
eurjchem-208	81	41	(	(	PUNCT
eurjchem-208	81	42	m+	m+	NUM
eurjchem-208	81	43	–	–	PUNCT
eurjchem-208	81	44	h	h	NOUN
eurjchem-208	81	45	,	,	PUNCT
eurjchem-208	81	46	15	15	NUM
eurjchem-208	81	47	%	%	NOUN
eurjchem-208	81	48	)	)	PUNCT
eurjchem-208	81	49	,	,	PUNCT
eurjchem-208	81	50	388	388	NUM
eurjchem-208	81	51	(	(	PUNCT
eurjchem-208	81	52	m+–2h	m+–2h	PROPN
eurjchem-208	81	53	,	,	PUNCT
eurjchem-208	81	54	30	30	NUM
eurjchem-208	81	55	)	)	PUNCT
eurjchem-208	81	56	,	,	PUNCT
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eurjchem-208	81	58	(	(	PUNCT
eurjchem-208	81	59	18	18	NUM
eurjchem-208	81	60	)	)	PUNCT
eurjchem-208	81	61	,	,	PUNCT
eurjchem-208	81	62	274	274	NUM
eurjchem-208	81	63	(	(	PUNCT
eurjchem-208	81	64	22	22	NUM
eurjchem-208	81	65	)	)	PUNCT
eurjchem-208	81	66	,	,	PUNCT
eurjchem-208	81	67	184	184	NUM
eurjchem-208	81	68	(	(	PUNCT
eurjchem-208	81	69	18	18	NUM
eurjchem-208	81	70	)	)	PUNCT
eurjchem-208	81	71	,	,	PUNCT
eurjchem-208	81	72	144	144	NUM
eurjchem-208	81	73	(	(	PUNCT
eurjchem-208	81	74	52	52	NUM
eurjchem-208	81	75	)	)	PUNCT
eurjchem-208	81	76	,	,	PUNCT
eurjchem-208	81	77	103	103	NUM
eurjchem-208	81	78	(	(	PUNCT
eurjchem-208	81	79	81	81	NUM
eurjchem-208	81	80	)	)	PUNCT
eurjchem-208	81	81	,	,	PUNCT
eurjchem-208	81	82	77	77	NUM
eurjchem-208	81	83	(	(	PUNCT
eurjchem-208	81	84	85	85	NUM
eurjchem-208	81	85	)	)	PUNCT
eurjchem-208	81	86	,	,	PUNCT
eurjchem-208	81	87	51	51	NUM
eurjchem-208	81	88	(	(	PUNCT
eurjchem-208	81	89	100	100	NUM
eurjchem-208	81	90	)	)	PUNCT
eurjchem-208	81	91	.	.	PUNCT
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eurjchem-208	82	2	.	.	PUNCT
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eurjchem-208	82	4	.	.	PUNCT
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eurjchem-208	83	3	(	(	PUNCT
eurjchem-208	83	4	390.34	390.34	NUM
eurjchem-208	83	5	):	):	PUNCT
eurjchem-208	83	6	c	c	X
eurjchem-208	83	7	,	,	PUNCT
eurjchem-208	83	8	61.54	61.54	NUM
eurjchem-208	83	9	;	;	PUNCT
eurjchem-208	83	10	h	h	NOUN
eurjchem-208	83	11	,	,	PUNCT
eurjchem-208	83	12	3.87	3.87	NUM
eurjchem-208	83	13	;	;	PUNCT
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eurjchem-208	83	15	,	,	PUNCT
eurjchem-208	83	16	14.35	14.35	NUM
eurjchem-208	83	17	.	.	PUNCT
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eurjchem-208	83	19	:	:	PUNCT
eurjchem-208	84	1	c	c	X
eurjchem-208	84	2	,	,	PUNCT
eurjchem-208	84	3	61.27	61.27	NUM
eurjchem-208	84	4	;	;	PUNCT
eurjchem-208	84	5	h	h	NOUN
eurjchem-208	84	6	,	,	PUNCT
eurjchem-208	84	7	3.67	3.67	NUM
eurjchem-208	84	8	;	;	PUNCT
eurjchem-208	84	9	n	n	CCONJ
eurjchem-208	84	10	,	,	PUNCT
eurjchem-208	84	11	13.96	13.96	NUM
eurjchem-208	84	12	%	%	NOUN
eurjchem-208	84	13	.	.	PUNCT
eurjchem-208	85	1	2.2.3.2	2.2.3.2	X
eurjchem-208	85	2	.	.	X
eurjchem-208	85	3	bis{3‐(4`‐biphenyl)‐4‐formyl‐1h‐pyrazol‐1‐yl	bis{3‐(4`‐biphenyl)‐4‐formyl‐1h‐pyrazol‐1‐yl	NOUN
eurjchem-208	85	4	}	}	PUNCT
eurjchem-208	85	5	phosphine	phosphine	NOUN
eurjchem-208	85	6	oxide	oxide	NOUN
eurjchem-208	85	7	(	(	PUNCT
eurjchem-208	85	8	4b	4b	X
eurjchem-208	85	9	)	)	PUNCT
eurjchem-208	85	10	orange	orange	PROPN
eurjchem-208	85	11	crystals	crystal	NOUN
eurjchem-208	85	12	from	from	ADP
eurjchem-208	85	13	ethanol	ethanol	NOUN
eurjchem-208	85	14	in	in	ADP
eurjchem-208	85	15	62	62	NUM
eurjchem-208	85	16	%	%	NOUN
eurjchem-208	85	17	yield	yield	NOUN
eurjchem-208	85	18	.	.	PUNCT
eurjchem-208	86	1	m.p	m.p	PROPN
eurjchem-208	86	2	.	.	PROPN
eurjchem-208	87	1	:	:	PUNCT
eurjchem-208	88	1	149–150	149–150	NUM
eurjchem-208	88	2	oc	oc	X
eurjchem-208	88	3	.	.	PUNCT
eurjchem-208	89	1	ir	ir	PROPN
eurjchem-208	89	2	(	(	PUNCT
eurjchem-208	89	3	kbr	kbr	PROPN
eurjchem-208	89	4	,	,	PUNCT
eurjchem-208	89	5	max	max	PROPN
eurjchem-208	89	6	,	,	PUNCT
eurjchem-208	89	7	cm‐1	cm‐1	PROPN
eurjchem-208	89	8	):	):	PUNCT
eurjchem-208	89	9	3054	3054	NUM
eurjchem-208	89	10	,	,	PUNCT
eurjchem-208	89	11	3029	3029	NUM
eurjchem-208	89	12	(	(	PUNCT
eurjchem-208	89	13	c	c	NOUN
eurjchem-208	89	14	–	–	PUNCT
eurjchem-208	89	15	harom	harom	NOUN
eurjchem-208	89	16	)	)	PUNCT
eurjchem-208	89	17	,	,	PUNCT
eurjchem-208	89	18	2363	2363	NUM
eurjchem-208	89	19	(	(	PUNCT
eurjchem-208	89	20	p	p	X
eurjchem-208	89	21	–	–	PUNCT
eurjchem-208	89	22	h	h	NOUN
eurjchem-208	89	23	)	)	PUNCT
eurjchem-208	89	24	,	,	PUNCT
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eurjchem-208	89	26	(	(	PUNCT
eurjchem-208	89	27	c	c	NOUN
eurjchem-208	89	28	=	=	NOUN
eurjchem-208	89	29	o	o	NOUN
eurjchem-208	89	30	)	)	PUNCT
eurjchem-208	89	31	,	,	PUNCT
eurjchem-208	89	32	1643	1643	NUM
eurjchem-208	89	33	(	(	PUNCT
eurjchem-208	89	34	c	c	NOUN
eurjchem-208	89	35	=	=	SYM
eurjchem-208	89	36	n	n	NUM
eurjchem-208	89	37	)	)	PUNCT
eurjchem-208	89	38	,	,	PUNCT
eurjchem-208	89	39	1601	1601	NUM
eurjchem-208	89	40	(	(	PUNCT
eurjchem-208	89	41	c	c	NOUN
eurjchem-208	89	42	=	=	SYM
eurjchem-208	89	43	c	c	NOUN
eurjchem-208	89	44	)	)	PUNCT
eurjchem-208	89	45	,	,	PUNCT
eurjchem-208	89	46	1241	1241	NUM
eurjchem-208	89	47	(	(	PUNCT
eurjchem-208	89	48	p	p	NOUN
eurjchem-208	89	49	=	=	NOUN
eurjchem-208	89	50	o	o	NOUN
eurjchem-208	89	51	)	)	PUNCT
eurjchem-208	89	52	.	.	PUNCT
eurjchem-208	90	1	1h	1h	NUM
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eurjchem-208	90	3	(	(	PUNCT
eurjchem-208	90	4	dmso	dmso	NOUN
eurjchem-208	90	5	,	,	PUNCT
eurjchem-208	90	6	δ	δ	PROPN
eurjchem-208	90	7	ppm	ppm	VERB
eurjchem-208	90	8	):	):	PUNCT
eurjchem-208	90	9	7.54	7.54	NUM
eurjchem-208	90	10	(	(	PUNCT
eurjchem-208	90	11	d	d	PROPN
eurjchem-208	90	12	,	,	PUNCT
eurjchem-208	90	13	1h	1h	NUM
eurjchem-208	90	14	,	,	PUNCT
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eurjchem-208	90	16	hz	hz	NOUN
eurjchem-208	90	17	,	,	PUNCT
eurjchem-208	90	18	p	p	NOUN
eurjchem-208	90	19	–	–	PUNCT
eurjchem-208	90	20	h	h	NOUN
eurjchem-208	90	21	)	)	PUNCT
eurjchem-208	90	22	,	,	PUNCT
eurjchem-208	90	23	7.47–8.14	7.47–8.14	NUM
eurjchem-208	90	24	(	(	PUNCT
eurjchem-208	90	25	m	m	PROPN
eurjchem-208	90	26	,	,	PUNCT
eurjchem-208	90	27	18h	18h	NOUN
eurjchem-208	90	28	,	,	PUNCT
eurjchem-208	90	29	ar−h	ar−h	NOUN
eurjchem-208	90	30	)	)	PUNCT
eurjchem-208	90	31	,	,	PUNCT
eurjchem-208	90	32	8.84	8.84	NUM
eurjchem-208	90	33	(	(	PUNCT
eurjchem-208	90	34	s	s	PROPN
eurjchem-208	90	35	,	,	PUNCT
eurjchem-208	90	36	2h	2h	NUM
eurjchem-208	90	37	,	,	PUNCT
eurjchem-208	90	38	c5	c5	PROPN
eurjchem-208	90	39	–	–	PUNCT
eurjchem-208	90	40	hpyrazole	hpyrazole	NOUN
eurjchem-208	90	41	)	)	PUNCT
eurjchem-208	90	42	,	,	PUNCT
eurjchem-208	90	43	10.00	10.00	NUM
eurjchem-208	90	44	(	(	PUNCT
eurjchem-208	90	45	s	s	PROPN
eurjchem-208	90	46	,	,	PUNCT
eurjchem-208	90	47	2h	2h	NUM
eurjchem-208	90	48	,	,	PUNCT
eurjchem-208	90	49	cho	cho	NOUN
eurjchem-208	90	50	)	)	PUNCT
eurjchem-208	90	51	.	.	PUNCT
eurjchem-208	91	1	31p	31p	NUM
eurjchem-208	91	2	nmr	nmr	NOUN
eurjchem-208	91	3	(	(	PUNCT
eurjchem-208	91	4	dmso	dmso	NOUN
eurjchem-208	91	5	,	,	PUNCT
eurjchem-208	91	6	δ	δ	PROPN
eurjchem-208	91	7	ppm	ppm	VERB
eurjchem-208	91	8	):	):	PUNCT
eurjchem-208	91	9	7.71	7.71	NUM
eurjchem-208	91	10	.	.	PUNCT
eurjchem-208	92	1	ms	ms	NOUN
eurjchem-208	92	2	(	(	PUNCT
eurjchem-208	92	3	m	m	PROPN
eurjchem-208	92	4	/	/	SYM
eurjchem-208	92	5	e	e	NOUN
eurjchem-208	92	6	,	,	PUNCT
eurjchem-208	92	7	%	%	INTJ
eurjchem-208	92	8	):	):	PUNCT
eurjchem-208	92	9	390	390	NUM
eurjchem-208	92	10	(	(	PUNCT
eurjchem-208	92	11	m+–c12h8	m+–c12h8	PROPN
eurjchem-208	92	12	,	,	PUNCT
eurjchem-208	92	13	32	32	NUM
eurjchem-208	92	14	%	%	NOUN
eurjchem-208	92	15	)	)	PUNCT
eurjchem-208	92	16	,	,	PUNCT
eurjchem-208	92	17	351	351	NUM
eurjchem-208	92	18	(	(	PUNCT
eurjchem-208	92	19	21	21	NUM
eurjchem-208	92	20	)	)	PUNCT
eurjchem-208	92	21	,	,	PUNCT
eurjchem-208	92	22	223	223	NUM
eurjchem-208	92	23	(	(	PUNCT
eurjchem-208	92	24	33	33	NUM
eurjchem-208	92	25	)	)	PUNCT
eurjchem-208	92	26	,	,	PUNCT
eurjchem-208	92	27	152	152	NUM
eurjchem-208	92	28	(	(	PUNCT
eurjchem-208	92	29	6	6	NUM
eurjchem-208	92	30	)	)	PUNCT
eurjchem-208	92	31	,	,	PUNCT
eurjchem-208	92	32	139	139	NUM
eurjchem-208	92	33	(	(	PUNCT
eurjchem-208	92	34	51	51	NUM
eurjchem-208	92	35	)	)	PUNCT
eurjchem-208	92	36	,	,	PUNCT
eurjchem-208	92	37	99	99	NUM
eurjchem-208	92	38	(	(	PUNCT
eurjchem-208	92	39	100	100	NUM
eurjchem-208	92	40	)	)	PUNCT
eurjchem-208	92	41	,	,	PUNCT
eurjchem-208	92	42	77	77	NUM
eurjchem-208	92	43	(	(	PUNCT
eurjchem-208	92	44	35	35	NUM
eurjchem-208	92	45	)	)	PUNCT
eurjchem-208	92	46	,	,	PUNCT
eurjchem-208	92	47	60	60	NUM
eurjchem-208	92	48	(	(	PUNCT
eurjchem-208	92	49	89	89	NUM
eurjchem-208	92	50	)	)	PUNCT
eurjchem-208	92	51	,	,	PUNCT
eurjchem-208	92	52	55	55	NUM
eurjchem-208	92	53	(	(	PUNCT
eurjchem-208	92	54	68	68	NUM
eurjchem-208	92	55	)	)	PUNCT
eurjchem-208	92	56	.	.	PUNCT
eurjchem-208	93	1	anal	anal	PROPN
eurjchem-208	93	2	.	.	PUNCT
eurjchem-208	93	3	calcd	calcd	NOUN
eurjchem-208	93	4	.	.	PUNCT
eurjchem-208	94	1	for	for	ADP
eurjchem-208	94	2	c32h23n4o3p	c32h23n4o3p	PROPN
eurjchem-208	94	3	(	(	PUNCT
eurjchem-208	94	4	542.54	542.54	NUM
eurjchem-208	94	5	):	):	PUNCT
eurjchem-208	94	6	c	c	X
eurjchem-208	94	7	,	,	PUNCT
eurjchem-208	94	8	70.84	70.84	NUM
eurjchem-208	94	9	;	;	PUNCT
eurjchem-208	94	10	h	h	X
eurjchem-208	94	11	,	,	PUNCT
eurjchem-208	94	12	4.27	4.27	NUM
eurjchem-208	94	13	;	;	PUNCT
eurjchem-208	94	14	n	n	CCONJ
eurjchem-208	94	15	,	,	PUNCT
eurjchem-208	94	16	10.33	10.33	NUM
eurjchem-208	94	17	.	.	PUNCT
eurjchem-208	94	18	found	find	VERB
eurjchem-208	94	19	:	:	PUNCT
eurjchem-208	95	1	c	c	X
eurjchem-208	95	2	,	,	PUNCT
eurjchem-208	95	3	70.53	70.53	NUM
eurjchem-208	95	4	;	;	PUNCT
eurjchem-208	95	5	h	h	NOUN
eurjchem-208	95	6	,	,	PUNCT
eurjchem-208	95	7	3.86	3.86	NUM
eurjchem-208	95	8	;	;	PUNCT
eurjchem-208	95	9	n	n	CCONJ
eurjchem-208	95	10	,	,	PUNCT
eurjchem-208	95	11	9.90	9.90	NUM
eurjchem-208	95	12	%	%	NOUN
eurjchem-208	95	13	.	.	PUNCT
eurjchem-208	96	1	2.2.3.3	2.2.3.3	NUM
eurjchem-208	96	2	.	.	PUNCT
eurjchem-208	97	1	bis{2,4‐dihydrochromeno[4,3‐c]pyrazol‐4‐hydroxy‐	bis{2,4‐dihydrochromeno[4,3‐c]pyrazol‐4‐hydroxy‐	NOUN
eurjchem-208	97	2	2‐yl}phosphine	2‐yl}phosphine	NUM
eurjchem-208	97	3	oxide	oxide	NOUN
eurjchem-208	97	4	(	(	PUNCT
eurjchem-208	97	5	6	6	NUM
eurjchem-208	97	6	)	)	PUNCT
eurjchem-208	97	7	red	red	ADJ
eurjchem-208	97	8	crystals	crystal	NOUN
eurjchem-208	97	9	from	from	ADP
eurjchem-208	97	10	ethanol	ethanol	NOUN
eurjchem-208	97	11	in	in	ADP
eurjchem-208	97	12	82	82	NUM
eurjchem-208	97	13	%	%	NOUN
eurjchem-208	97	14	yield	yield	NOUN
eurjchem-208	97	15	.	.	PUNCT
eurjchem-208	98	1	m.p	m.p	PROPN
eurjchem-208	98	2	.	.	PROPN
eurjchem-208	98	3	:	:	PUNCT
eurjchem-208	99	1	279–282	279–282	NUM
eurjchem-208	99	2	oc	oc	NOUN
eurjchem-208	99	3	.	.	PROPN
eurjchem-208	99	4	ir	ir	PROPN
eurjchem-208	99	5	(	(	PUNCT
eurjchem-208	99	6	kbr	kbr	PROPN
eurjchem-208	99	7	,	,	PUNCT
eurjchem-208	99	8	max	max	PROPN
eurjchem-208	99	9	,	,	PUNCT
eurjchem-208	99	10	cm‐1	cm‐1	NUM
eurjchem-208	99	11	):	):	PUNCT
eurjchem-208	99	12	3135	3135	NUM
eurjchem-208	99	13	(	(	PUNCT
eurjchem-208	99	14	br	br	PROPN
eurjchem-208	99	15	,	,	PUNCT
eurjchem-208	99	16	oh	oh	INTJ
eurjchem-208	99	17	)	)	PUNCT
eurjchem-208	99	18	,	,	PUNCT
eurjchem-208	99	19	3070	3070	NUM
eurjchem-208	99	20	(	(	PUNCT
eurjchem-208	99	21	c	c	X
eurjchem-208	99	22	–	–	PUNCT
eurjchem-208	99	23	harom	harom	NOUN
eurjchem-208	99	24	)	)	PUNCT
eurjchem-208	99	25	,	,	PUNCT
eurjchem-208	99	26	2930	2930	NUM
eurjchem-208	99	27	(	(	PUNCT
eurjchem-208	99	28	c	c	X
eurjchem-208	99	29	–	–	PUNCT
eurjchem-208	99	30	haliph	haliph	NOUN
eurjchem-208	99	31	)	)	PUNCT
eurjchem-208	99	32	,	,	PUNCT
eurjchem-208	99	33	2500	2500	NUM
eurjchem-208	99	34	(	(	PUNCT
eurjchem-208	99	35	p	p	X
eurjchem-208	99	36	–	–	PUNCT
eurjchem-208	99	37	h	h	NOUN
eurjchem-208	99	38	)	)	PUNCT
eurjchem-208	99	39	,	,	PUNCT
eurjchem-208	99	40	1656	1656	NUM
eurjchem-208	99	41	(	(	PUNCT
eurjchem-208	99	42	c	c	NOUN
eurjchem-208	99	43	=	=	SYM
eurjchem-208	99	44	n	n	NUM
eurjchem-208	99	45	)	)	PUNCT
eurjchem-208	99	46	,	,	PUNCT
eurjchem-208	99	47	1615	1615	NUM
eurjchem-208	99	48	(	(	PUNCT
eurjchem-208	99	49	c	c	X
eurjchem-208	99	50	=	=	SYM
eurjchem-208	99	51	c	c	NOUN
eurjchem-208	99	52	)	)	PUNCT
eurjchem-208	99	53	,	,	PUNCT
eurjchem-208	99	54	1246	1246	NUM
eurjchem-208	99	55	(	(	PUNCT
eurjchem-208	99	56	p	p	NOUN
eurjchem-208	99	57	=	=	NOUN
eurjchem-208	99	58	o	o	NOUN
eurjchem-208	99	59	)	)	PUNCT
eurjchem-208	99	60	,	,	PUNCT
eurjchem-208	99	61	1104	1104	NUM
eurjchem-208	99	62	(	(	PUNCT
eurjchem-208	99	63	c	c	X
eurjchem-208	99	64	–	–	PUNCT
eurjchem-208	99	65	o	o	NOUN
eurjchem-208	99	66	–	–	PUNCT
eurjchem-208	99	67	c	c	NOUN
eurjchem-208	99	68	)	)	PUNCT
eurjchem-208	99	69	.	.	PUNCT
eurjchem-208	100	1	1h	1h	NUM
eurjchem-208	100	2	nmr	nmr	NOUN
eurjchem-208	100	3	(	(	PUNCT
eurjchem-208	100	4	dmso	dmso	NOUN
eurjchem-208	100	5	,	,	PUNCT
eurjchem-208	100	6	δ	δ	PROPN
eurjchem-208	100	7	ppm	ppm	VERB
eurjchem-208	100	8	):	):	PUNCT
eurjchem-208	100	9	3.72	3.72	NUM
eurjchem-208	100	10	(	(	PUNCT
eurjchem-208	100	11	br	br	PROPN
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eurjchem-208	100	13	2h	2h	NUM
eurjchem-208	100	14	,	,	PUNCT
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eurjchem-208	100	18	d2o	d2o	NOUN
eurjchem-208	100	19	)	)	PUNCT
eurjchem-208	100	20	,	,	PUNCT
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eurjchem-208	100	22	(	(	PUNCT
eurjchem-208	100	23	s	s	PROPN
eurjchem-208	100	24	,	,	PUNCT
eurjchem-208	100	25	2h	2h	NUM
eurjchem-208	100	26	,	,	PUNCT
eurjchem-208	100	27	c2	c2	PROPN
eurjchem-208	100	28	–	–	PUNCT
eurjchem-208	100	29	hpyran),6.95–7.78	hpyran),6.95–7.78	PROPN
eurjchem-208	100	30	(	(	PUNCT
eurjchem-208	100	31	m	m	PROPN
eurjchem-208	100	32	,	,	PUNCT
eurjchem-208	100	33	8h	8h	PROPN
eurjchem-208	100	34	,	,	PUNCT
eurjchem-208	100	35	ar−h),7.44	ar−h),7.44	VERB
eurjchem-208	100	36	(	(	PUNCT
eurjchem-208	100	37	d	d	NOUN
eurjchem-208	100	38	,	,	PUNCT
eurjchem-208	100	39	1h	1h	NUM
eurjchem-208	100	40	,	,	PUNCT
eurjchem-208	100	41	jph=423	jph=423	NOUN
eurjchem-208	100	42	hz	hz	PROPN
eurjchem-208	100	43	,	,	PUNCT
eurjchem-208	100	44	p	p	NOUN
eurjchem-208	100	45	–	–	PUNCT
eurjchem-208	100	46	h	h	NOUN
eurjchem-208	100	47	)	)	PUNCT
eurjchem-208	100	48	,	,	PUNCT
eurjchem-208	100	49	7.96	7.96	NUM
eurjchem-208	100	50	(	(	PUNCT
eurjchem-208	100	51	s	s	PROPN
eurjchem-208	100	52	,	,	PUNCT
eurjchem-208	100	53	2h	2h	NUM
eurjchem-208	100	54	,	,	PUNCT
eurjchem-208	100	55	c5	c5	PROPN
eurjchem-208	100	56	–	–	PUNCT
eurjchem-208	100	57	hpyrazole	hpyrazole	NOUN
eurjchem-208	100	58	)	)	PUNCT
eurjchem-208	100	59	.	.	PUNCT
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eurjchem-208	101	2	.	.	PUNCT
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eurjchem-208	101	4	.	.	PUNCT
eurjchem-208	102	1	for	for	ADP
eurjchem-208	102	2	c20h15n4o5p	c20h15n4o5p	NUM
eurjchem-208	102	3	(	(	PUNCT
eurjchem-208	102	4	422.34	422.34	NUM
eurjchem-208	102	5	):	):	PUNCT
eurjchem-208	102	6	c	c	X
eurjchem-208	102	7	,	,	PUNCT
eurjchem-208	102	8	56.88	56.88	NUM
eurjchem-208	102	9	;	;	PUNCT
eurjchem-208	102	10	h	h	NOUN
eurjchem-208	102	11	,	,	PUNCT
eurjchem-208	102	12	3.58	3.58	NUM
eurjchem-208	102	13	;	;	PUNCT
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eurjchem-208	102	15	,	,	PUNCT
eurjchem-208	102	16	13.27	13.27	NUM
eurjchem-208	102	17	.	.	PUNCT
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eurjchem-208	102	19	:	:	PUNCT
eurjchem-208	103	1	c	c	X
eurjchem-208	103	2	,	,	PUNCT
eurjchem-208	103	3	56.56	56.56	NUM
eurjchem-208	103	4	;	;	PUNCT
eurjchem-208	103	5	h	h	NOUN
eurjchem-208	103	6	,	,	PUNCT
eurjchem-208	103	7	3.29	3.29	NUM
eurjchem-208	103	8	;	;	PUNCT
eurjchem-208	103	9	n	n	CCONJ
eurjchem-208	103	10	,	,	PUNCT
eurjchem-208	103	11	12.89	12.89	NUM
eurjchem-208	103	12	%	%	NOUN
eurjchem-208	103	13	.	.	PUNCT
eurjchem-208	104	1	2.2.3.4	2.2.3.4	NUM
eurjchem-208	104	2	.	.	PUNCT
eurjchem-208	104	3	bis{chromeno[2,3‐g]indazol‐11‐oxo‐2‐yl}phosphine	bis{chromeno[2,3‐g]indazol‐11‐oxo‐2‐yl}phosphine	NUM
eurjchem-208	104	4	oxide	oxide	NOUN
eurjchem-208	104	5	(	(	PUNCT
eurjchem-208	104	6	8)	8)	NUM
eurjchem-208	104	7	yellow	yellow	ADJ
eurjchem-208	104	8	crystals	crystal	NOUN
eurjchem-208	104	9	from	from	ADP
eurjchem-208	104	10	dilute	dilute	NOUN
eurjchem-208	104	11	dimethylformamide	dimethylformamide	NOUN
eurjchem-208	104	12	in	in	ADP
eurjchem-208	104	13	39	39	NUM
eurjchem-208	104	14	%	%	NOUN
eurjchem-208	104	15	yield	yield	NOUN
eurjchem-208	104	16	.	.	PUNCT
eurjchem-208	105	1	m.p	m.p	PROPN
eurjchem-208	105	2	.	.	PROPN
eurjchem-208	105	3	:	:	PUNCT
eurjchem-208	106	1	296–297	296–297	NUM
eurjchem-208	106	2	oc	oc	NOUN
eurjchem-208	106	3	.	.	PUNCT
eurjchem-208	106	4	ir	ir	PROPN
eurjchem-208	106	5	(	(	PUNCT
eurjchem-208	106	6	kbr	kbr	PROPN
eurjchem-208	106	7	,	,	PUNCT
eurjchem-208	106	8	max	max	PROPN
eurjchem-208	106	9	,	,	PUNCT
eurjchem-208	106	10	cm‐1	cm‐1	PROPN
eurjchem-208	106	11	):	):	PUNCT
eurjchem-208	106	12	3050	3050	NUM
eurjchem-208	106	13	(	(	PUNCT
eurjchem-208	106	14	c	c	X
eurjchem-208	106	15	–	–	PUNCT
eurjchem-208	106	16	harom	harom	NOUN
eurjchem-208	106	17	)	)	PUNCT
eurjchem-208	106	18	,	,	PUNCT
eurjchem-208	106	19	2642	2642	NUM
eurjchem-208	106	20	(	(	PUNCT
eurjchem-208	106	21	p	p	NOUN
eurjchem-208	106	22	–	–	PUNCT
eurjchem-208	106	23	h	h	NOUN
eurjchem-208	106	24	)	)	PUNCT
eurjchem-208	106	25	,	,	PUNCT
eurjchem-208	106	26	1646	1646	NUM
eurjchem-208	106	27	(	(	PUNCT
eurjchem-208	106	28	c	c	NOUN
eurjchem-208	106	29	=	=	NOUN
eurjchem-208	106	30	o	o	NOUN
eurjchem-208	106	31	)	)	PUNCT
eurjchem-208	106	32	,	,	PUNCT
eurjchem-208	106	33	1596	1596	NUM
eurjchem-208	106	34	(	(	PUNCT
eurjchem-208	106	35	c	c	NOUN
eurjchem-208	106	36	=	=	SYM
eurjchem-208	106	37	n	n	NUM
eurjchem-208	106	38	)	)	PUNCT
eurjchem-208	106	39	,	,	PUNCT
eurjchem-208	106	40	1569	1569	NUM
eurjchem-208	106	41	(	(	PUNCT
eurjchem-208	106	42	c	c	X
eurjchem-208	106	43	=	=	SYM
eurjchem-208	106	44	c	c	NOUN
eurjchem-208	106	45	)	)	PUNCT
eurjchem-208	106	46	,	,	PUNCT
eurjchem-208	106	47	1246	1246	NUM
eurjchem-208	106	48	(	(	PUNCT
eurjchem-208	106	49	p	p	NOUN
eurjchem-208	106	50	=	=	NOUN
eurjchem-208	106	51	o	o	NOUN
eurjchem-208	106	52	)	)	PUNCT
eurjchem-208	106	53	,	,	PUNCT
eurjchem-208	106	54	1041	1041	NUM
eurjchem-208	106	55	(	(	PUNCT
eurjchem-208	106	56	c	c	X
eurjchem-208	106	57	–	–	PUNCT
eurjchem-208	106	58	o	o	NOUN
eurjchem-208	106	59	–	–	PUNCT
eurjchem-208	106	60	c	c	NOUN
eurjchem-208	106	61	)	)	PUNCT
eurjchem-208	106	62	.	.	PUNCT
eurjchem-208	107	1	1h	1h	NUM
eurjchem-208	107	2	nmr	nmr	NOUN
eurjchem-208	107	3	(	(	PUNCT
eurjchem-208	107	4	dmso	dmso	NOUN
eurjchem-208	107	5	,	,	PUNCT
eurjchem-208	107	6	δ	δ	PROPN
eurjchem-208	107	7	ppm):6.50	ppm):6.50	PROPN
eurjchem-208	107	8	(	(	PUNCT
eurjchem-208	107	9	d	d	PROPN
eurjchem-208	107	10	,	,	PUNCT
eurjchem-208	107	11	1h	1h	NUM
eurjchem-208	107	12	,	,	PUNCT
eurjchem-208	107	13	jph=556	jph=556	NOUN
eurjchem-208	107	14	hz	hz	PROPN
eurjchem-208	107	15	,	,	PUNCT
eurjchem-208	107	16	p	p	NOUN
eurjchem-208	107	17	–	–	PUNCT
eurjchem-208	107	18	h	h	NOUN
eurjchem-208	107	19	)	)	PUNCT
eurjchem-208	107	20	,	,	PUNCT
eurjchem-208	107	21	7.05–7.80	7.05–7.80	NUM
eurjchem-208	107	22	(	(	PUNCT
eurjchem-208	107	23	m	m	PROPN
eurjchem-208	107	24	,	,	PUNCT
eurjchem-208	107	25	12h	12h	NUM
eurjchem-208	107	26	,	,	PUNCT
eurjchem-208	107	27	ar−h	ar−h	NOUN
eurjchem-208	107	28	)	)	PUNCT
eurjchem-208	107	29	,	,	PUNCT
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eurjchem-208	107	33	,	,	PUNCT
eurjchem-208	107	34	2h	2h	NUM
eurjchem-208	107	35	,	,	PUNCT
eurjchem-208	107	36	c5	c5	PROPN
eurjchem-208	107	37	–	–	PUNCT
eurjchem-208	107	38	hpyrazole	hpyrazole	NOUN
eurjchem-208	107	39	)	)	PUNCT
eurjchem-208	107	40	.	.	PUNCT
eurjchem-208	108	1	ms	ms	NOUN
eurjchem-208	108	2	(	(	PUNCT
eurjchem-208	108	3	m	m	PROPN
eurjchem-208	108	4	/	/	SYM
eurjchem-208	108	5	e	e	NOUN
eurjchem-208	108	6	,	,	PUNCT
eurjchem-208	108	7	%	%	INTJ
eurjchem-208	108	8	):	):	PUNCT
eurjchem-208	108	9	518	518	NUM
eurjchem-208	108	10	(	(	PUNCT
eurjchem-208	108	11	m+	m+	NUM
eurjchem-208	108	12	,	,	PUNCT
eurjchem-208	108	13	2	2	NUM
eurjchem-208	108	14	%	%	NOUN
eurjchem-208	108	15	)	)	PUNCT
eurjchem-208	108	16	,	,	PUNCT
eurjchem-208	108	17	458	458	NUM
eurjchem-208	108	18	(	(	PUNCT
eurjchem-208	108	19	3	3	NUM
eurjchem-208	108	20	)	)	PUNCT
eurjchem-208	108	21	,	,	PUNCT
eurjchem-208	108	22	384	384	NUM
eurjchem-208	108	23	(	(	PUNCT
eurjchem-208	108	24	100	100	NUM
eurjchem-208	108	25	)	)	PUNCT
eurjchem-208	108	26	,	,	PUNCT
eurjchem-208	108	27	369	369	NUM
eurjchem-208	108	28	(	(	PUNCT
eurjchem-208	108	29	83	83	NUM
eurjchem-208	108	30	)	)	PUNCT
eurjchem-208	108	31	,	,	PUNCT
eurjchem-208	108	32	284	284	NUM
eurjchem-208	108	33	(	(	PUNCT
eurjchem-208	108	34	2	2	NUM
eurjchem-208	108	35	)	)	PUNCT
eurjchem-208	108	36	,	,	PUNCT
eurjchem-208	108	37	192	192	NUM
eurjchem-208	108	38	(	(	PUNCT
eurjchem-208	108	39	74	74	NUM
eurjchem-208	108	40	)	)	PUNCT
eurjchem-208	108	41	,	,	PUNCT
eurjchem-208	108	42	165	165	NUM
eurjchem-208	108	43	(	(	PUNCT
eurjchem-208	108	44	6	6	NUM
eurjchem-208	108	45	)	)	PUNCT
eurjchem-208	108	46	,	,	PUNCT
eurjchem-208	108	47	120	120	NUM
eurjchem-208	108	48	(	(	PUNCT
eurjchem-208	108	49	10	10	NUM
eurjchem-208	108	50	)	)	PUNCT
eurjchem-208	108	51	,	,	PUNCT
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eurjchem-208	108	53	(	(	PUNCT
eurjchem-208	108	54	2	2	NUM
eurjchem-208	108	55	)	)	PUNCT
eurjchem-208	108	56	,	,	PUNCT
eurjchem-208	108	57	92	92	NUM
eurjchem-208	108	58	(	(	PUNCT
eurjchem-208	108	59	7	7	NUM
eurjchem-208	108	60	)	)	PUNCT
eurjchem-208	108	61	,	,	PUNCT
eurjchem-208	108	62	77	77	NUM
eurjchem-208	108	63	(	(	PUNCT
eurjchem-208	108	64	30	30	NUM
eurjchem-208	108	65	)	)	PUNCT
eurjchem-208	108	66	,	,	PUNCT
eurjchem-208	108	67	69	69	NUM
eurjchem-208	108	68	(	(	PUNCT
eurjchem-208	108	69	35	35	NUM
eurjchem-208	108	70	)	)	PUNCT
eurjchem-208	108	71	,	,	PUNCT
eurjchem-208	108	72	53	53	NUM
eurjchem-208	108	73	(	(	PUNCT
eurjchem-208	108	74	19	19	NUM
eurjchem-208	108	75	)	)	PUNCT
eurjchem-208	108	76	.	.	PUNCT
eurjchem-208	109	1	anal	anal	PROPN
eurjchem-208	109	2	.	.	PUNCT
eurjchem-208	109	3	calcd	calcd	NOUN
eurjchem-208	109	4	.	.	PUNCT
eurjchem-208	110	1	forc28h15n4o5p	forc28h15n4o5p	PUNCT
eurjchem-208	111	1	(	(	PUNCT
eurjchem-208	111	2	518.43	518.43	NUM
eurjchem-208	111	3	):	):	PUNCT
eurjchem-208	111	4	c	c	X
eurjchem-208	111	5	,	,	PUNCT
eurjchem-208	111	6	64.87	64.87	NUM
eurjchem-208	111	7	;	;	PUNCT
eurjchem-208	111	8	h	h	X
eurjchem-208	111	9	,	,	PUNCT
eurjchem-208	111	10	2.92	2.92	NUM
eurjchem-208	111	11	;	;	PUNCT
eurjchem-208	111	12	n	n	CCONJ
eurjchem-208	111	13	,	,	PUNCT
eurjchem-208	111	14	10.81	10.81	NUM
eurjchem-208	111	15	.	.	PUNCT
eurjchem-208	112	1	found	find	VERB
eurjchem-208	112	2	:	:	PUNCT
eurjchem-208	113	1	c	c	X
eurjchem-208	113	2	,	,	PUNCT
eurjchem-208	113	3	64.63	64.63	NUM
eurjchem-208	113	4	;	;	PUNCT
eurjchem-208	113	5	h	h	NOUN
eurjchem-208	113	6	,	,	PUNCT
eurjchem-208	113	7	2.71	2.71	NUM
eurjchem-208	113	8	;	;	PUNCT
eurjchem-208	113	9	n	n	CCONJ
eurjchem-208	113	10	,	,	PUNCT
eurjchem-208	113	11	10.52	10.52	NUM
eurjchem-208	113	12	%	%	NOUN
eurjchem-208	113	13	.	.	PUNCT
eurjchem-208	114	1	2.2.4	2.2.4	X
eurjchem-208	114	2	.	.	X
eurjchem-208	114	3	synthesis	synthesis	NOUN
eurjchem-208	114	4	of	of	ADP
eurjchem-208	114	5	bis(4‐carboxypyrazolyl)phosphine	bis(4‐carboxypyrazolyl)phosphine	ADJ
eurjchem-208	114	6	oxides	oxide	NOUN
eurjchem-208	114	7	(	(	PUNCT
eurjchem-208	114	8	5a	5a	NUM
eurjchem-208	114	9	,	,	PUNCT
eurjchem-208	114	10	5b	5b	NUM
eurjchem-208	114	11	):	):	PUNCT
eurjchem-208	114	12	general	general	ADJ
eurjchem-208	114	13	procedure	procedure	NOUN
eurjchem-208	114	14	for	for	ADP
eurjchem-208	114	15	oxidation	oxidation	NOUN
eurjchem-208	114	16	of	of	ADP
eurjchem-208	114	17	bis‐(4‐formyl	bis‐(4‐formyl	PROPN
eurjchem-208	114	18	pyrazolyl)phosphine	pyrazolyl)phosphine	NOUN
eurjchem-208	114	19	oxides	oxide	NOUN
eurjchem-208	114	20	(	(	PUNCT
eurjchem-208	114	21	4a	4a	NUM
eurjchem-208	114	22	,	,	PUNCT
eurjchem-208	114	23	4b	4b	X
eurjchem-208	114	24	)	)	PUNCT
eurjchem-208	114	25	abdel‐aziz	abdel‐aziz	NOUN
eurjchem-208	115	1	et	et	PROPN
eurjchem-208	115	2	al./	al./	ADV
eurjchem-208	115	3	european	european	PROPN
eurjchem-208	115	4	journal	journal	PROPN
eurjchem-208	115	5	of	of	ADP
eurjchem-208	115	6	chemistry	chemistry	NOUN
eurjchem-208	115	7	2	2	NUM
eurjchem-208	115	8	(	(	PUNCT
eurjchem-208	115	9	1	1	NUM
eurjchem-208	115	10	)	)	PUNCT
eurjchem-208	115	11	(	(	PUNCT
eurjchem-208	115	12	2011	2011	NUM
eurjchem-208	115	13	)	)	PUNCT
eurjchem-208	115	14	25‐35	25‐35	NUM
eurjchem-208	115	15	27	27	NUM
eurjchem-208	115	16	scheme	scheme	NOUN
eurjchem-208	115	17	1	1	NUM
eurjchem-208	115	18	a	a	DET
eurjchem-208	115	19	solution	solution	NOUN
eurjchem-208	115	20	of	of	ADP
eurjchem-208	115	21	potassium	potassium	NOUN
eurjchem-208	115	22	permanganate	permanganate	NOUN
eurjchem-208	115	23	(	(	PUNCT
eurjchem-208	115	24	0.002	0.002	NUM
eurjchem-208	115	25	mol	mol	NOUN
eurjchem-208	115	26	,	,	PUNCT
eurjchem-208	115	27	0.32	0.32	NUM
eurjchem-208	115	28	g	g	NOUN
eurjchem-208	115	29	)	)	PUNCT
eurjchem-208	115	30	in	in	ADP
eurjchem-208	115	31	water	water	NOUN
eurjchem-208	115	32	(	(	PUNCT
eurjchem-208	115	33	10	10	NUM
eurjchem-208	115	34	cm3	cm3	NOUN
eurjchem-208	115	35	)	)	PUNCT
eurjchem-208	115	36	was	be	AUX
eurjchem-208	115	37	added	add	VERB
eurjchem-208	115	38	with	with	ADP
eurjchem-208	115	39	stirring	stir	VERB
eurjchem-208	115	40	to	to	ADP
eurjchem-208	115	41	a	a	DET
eurjchem-208	115	42	suspension	suspension	NOUN
eurjchem-208	115	43	of	of	ADP
eurjchem-208	115	44	bis‐(4‐formylpyrazolyl)phosphine	bis‐(4‐formylpyrazolyl)phosphine	NOUN
eurjchem-208	115	45	oxides	oxide	NOUN
eurjchem-208	115	46	4a	4a	NOUN
eurjchem-208	115	47	,	,	PUNCT
eurjchem-208	115	48	b	b	PROPN
eurjchem-208	115	49	(	(	PUNCT
eurjchem-208	115	50	0.001	0.001	NUM
eurjchem-208	115	51	mol	mol	NOUN
eurjchem-208	115	52	)	)	PUNCT
eurjchem-208	115	53	in	in	ADP
eurjchem-208	115	54	pyridine	pyridine	NOUN
eurjchem-208	115	55	(	(	PUNCT
eurjchem-208	115	56	10	10	NUM
eurjchem-208	115	57	cm3	cm3	NOUN
eurjchem-208	115	58	)	)	PUNCT
eurjchem-208	115	59	at	at	ADP
eurjchem-208	115	60	room	room	NOUN
eurjchem-208	115	61	temperature	temperature	NOUN
eurjchem-208	115	62	.	.	PUNCT
eurjchem-208	116	1	the	the	DET
eurjchem-208	116	2	reaction	reaction	NOUN
eurjchem-208	116	3	mixture	mixture	NOUN
eurjchem-208	116	4	was	be	AUX
eurjchem-208	116	5	stirred	stir	VERB
eurjchem-208	116	6	for	for	ADP
eurjchem-208	116	7	3	3	NUM
eurjchem-208	116	8	h	h	NOUN
eurjchem-208	116	9	,	,	PUNCT
eurjchem-208	116	10	a	a	DET
eurjchem-208	116	11	solution	solution	NOUN
eurjchem-208	116	12	of	of	ADP
eurjchem-208	116	13	naoh	naoh	NOUN
eurjchem-208	116	14	(	(	PUNCT
eurjchem-208	116	15	1	1	NUM
eurjchem-208	116	16	%	%	NOUN
eurjchem-208	116	17	,	,	PUNCT
eurjchem-208	116	18	10	10	NUM
eurjchem-208	116	19	cm3	cm3	NOUN
eurjchem-208	116	20	)	)	PUNCT
eurjchem-208	116	21	was	be	AUX
eurjchem-208	116	22	added	add	VERB
eurjchem-208	116	23	,	,	PUNCT
eurjchem-208	116	24	and	and	CCONJ
eurjchem-208	116	25	stirring	stir	VERB
eurjchem-208	116	26	continued	continue	VERB
eurjchem-208	116	27	for	for	ADP
eurjchem-208	116	28	2	2	NUM
eurjchem-208	116	29	h	h	NOUN
eurjchem-208	116	30	at	at	ADP
eurjchem-208	116	31	50	50	NUM
eurjchem-208	116	32	°	°	NOUN
eurjchem-208	116	33	c	c	NOUN
eurjchem-208	116	34	.	.	PUNCT
eurjchem-208	117	1	after	after	ADP
eurjchem-208	117	2	cooling	cool	VERB
eurjchem-208	117	3	,	,	PUNCT
eurjchem-208	117	4	the	the	DET
eurjchem-208	117	5	inorganic	inorganic	ADJ
eurjchem-208	117	6	precipitate	precipitate	NOUN
eurjchem-208	117	7	was	be	AUX
eurjchem-208	117	8	filtered	filter	VERB
eurjchem-208	117	9	off	off	ADP
eurjchem-208	117	10	and	and	CCONJ
eurjchem-208	117	11	washed	wash	VERB
eurjchem-208	117	12	with	with	ADP
eurjchem-208	117	13	water	water	NOUN
eurjchem-208	117	14	.	.	PUNCT
eurjchem-208	118	1	the	the	DET
eurjchem-208	118	2	filtrate	filtrate	NOUN
eurjchem-208	118	3	was	be	AUX
eurjchem-208	118	4	acidified	acidify	VERB
eurjchem-208	118	5	with	with	ADP
eurjchem-208	118	6	hydrochloric	hydrochloric	ADJ
eurjchem-208	118	7	acid	acid	NOUN
eurjchem-208	118	8	to	to	ADP
eurjchem-208	118	9	ph	ph	ADJ
eurjchem-208	118	10	=	=	NOUN
eurjchem-208	118	11	4	4	NUM
eurjchem-208	118	12	.	.	PUNCT
eurjchem-208	119	1	the	the	DET
eurjchem-208	119	2	formed	form	VERB
eurjchem-208	119	3	precipitate	precipitate	NOUN
eurjchem-208	119	4	was	be	AUX
eurjchem-208	119	5	filtered	filter	VERB
eurjchem-208	119	6	off	off	ADP
eurjchem-208	119	7	,	,	PUNCT
eurjchem-208	119	8	washed	wash	VERB
eurjchem-208	119	9	with	with	ADP
eurjchem-208	119	10	water	water	NOUN
eurjchem-208	119	11	,	,	PUNCT
eurjchem-208	119	12	dried	dry	VERB
eurjchem-208	119	13	,	,	PUNCT
eurjchem-208	119	14	and	and	CCONJ
eurjchem-208	119	15	crystallized	crystallize	VERB
eurjchem-208	119	16	from	from	ADP
eurjchem-208	119	17	dilute	dilute	NOUN
eurjchem-208	119	18	ethanol	ethanol	NOUN
eurjchem-208	119	19	.	.	PUNCT
eurjchem-208	120	1	2.2.4.1	2.2.4.1	NUM
eurjchem-208	120	2	.	.	X
eurjchem-208	120	3	bis{4‐carboxy‐3‐phenyl‐1h‐pyrazol‐1‐yl}phosphine	bis{4‐carboxy‐3‐phenyl‐1h‐pyrazol‐1‐yl}phosphine	PROPN
eurjchem-208	120	4	oxide	oxide	NOUN
eurjchem-208	120	5	(	(	PUNCT
eurjchem-208	120	6	5a	5a	NUM
eurjchem-208	120	7	)	)	PUNCT
eurjchem-208	120	8	grey	grey	ADJ
eurjchem-208	120	9	crystals	crystal	NOUN
eurjchem-208	120	10	from	from	ADP
eurjchem-208	120	11	dilute	dilute	NOUN
eurjchem-208	120	12	ethanol	ethanol	NOUN
eurjchem-208	120	13	in	in	ADP
eurjchem-208	120	14	80	80	NUM
eurjchem-208	120	15	%	%	NOUN
eurjchem-208	120	16	yield	yield	NOUN
eurjchem-208	120	17	.	.	PUNCT
eurjchem-208	121	1	m.p	m.p	PROPN
eurjchem-208	121	2	.	.	PROPN
eurjchem-208	121	3	:	:	PUNCT
eurjchem-208	122	1	>	>	PUNCT
eurjchem-208	122	2	300	300	NUM
eurjchem-208	122	3	°	°	NOUN
eurjchem-208	122	4	c	c	NOUN
eurjchem-208	122	5	.	.	PUNCT
eurjchem-208	123	1	ir	ir	PROPN
eurjchem-208	123	2	(	(	PUNCT
eurjchem-208	123	3	kbr	kbr	PROPN
eurjchem-208	123	4	,	,	PUNCT
eurjchem-208	123	5	max	max	PROPN
eurjchem-208	123	6	,	,	PUNCT
eurjchem-208	123	7	cm‐1	cm‐1	PROPN
eurjchem-208	123	8	):	):	PUNCT
eurjchem-208	123	9	3243	3243	NUM
eurjchem-208	123	10	(	(	PUNCT
eurjchem-208	123	11	oh	oh	INTJ
eurjchem-208	123	12	)	)	PUNCT
eurjchem-208	123	13	,	,	PUNCT
eurjchem-208	123	14	2362	2362	NUM
eurjchem-208	123	15	(	(	PUNCT
eurjchem-208	123	16	p	p	X
eurjchem-208	123	17	–	–	PUNCT
eurjchem-208	123	18	h	h	NOUN
eurjchem-208	123	19	)	)	PUNCT
eurjchem-208	123	20	,	,	PUNCT
eurjchem-208	123	21	1713	1713	NUM
eurjchem-208	123	22	(	(	PUNCT
eurjchem-208	123	23	c	c	NOUN
eurjchem-208	123	24	=	=	NOUN
eurjchem-208	123	25	o	o	NOUN
eurjchem-208	123	26	)	)	PUNCT
eurjchem-208	123	27	,	,	PUNCT
eurjchem-208	123	28	1550	1550	NUM
eurjchem-208	123	29	(	(	PUNCT
eurjchem-208	123	30	c	c	NOUN
eurjchem-208	123	31	=	=	SYM
eurjchem-208	123	32	n	n	NUM
eurjchem-208	123	33	)	)	PUNCT
eurjchem-208	123	34	,	,	PUNCT
eurjchem-208	123	35	1237	1237	NUM
eurjchem-208	123	36	(	(	PUNCT
eurjchem-208	123	37	p	p	NOUN
eurjchem-208	123	38	=	=	NOUN
eurjchem-208	123	39	o	o	NOUN
eurjchem-208	123	40	)	)	PUNCT
eurjchem-208	123	41	.	.	PUNCT
eurjchem-208	124	1	1h	1h	NUM
eurjchem-208	124	2	nmr	nmr	NOUN
eurjchem-208	124	3	(	(	PUNCT
eurjchem-208	124	4	dmso	dmso	NOUN
eurjchem-208	124	5	,	,	PUNCT
eurjchem-208	124	6	δ	δ	PROPN
eurjchem-208	124	7	ppm	ppm	VERB
eurjchem-208	124	8	):	):	PUNCT
eurjchem-208	124	9	7.64	7.64	NUM
eurjchem-208	124	10	(	(	PUNCT
eurjchem-208	124	11	d	d	PROPN
eurjchem-208	124	12	,	,	PUNCT
eurjchem-208	124	13	1h	1h	NUM
eurjchem-208	124	14	,	,	PUNCT
eurjchem-208	124	15	jph=517	jph=517	PROPN
eurjchem-208	124	16	hz	hz	VERB
eurjchem-208	124	17	,	,	PUNCT
eurjchem-208	124	18	p	p	NOUN
eurjchem-208	124	19	–	–	PUNCT
eurjchem-208	124	20	h	h	NOUN
eurjchem-208	124	21	)	)	PUNCT
eurjchem-208	124	22	,	,	PUNCT
eurjchem-208	124	23	7.60–8.17(m	7.60–8.17(m	NUM
eurjchem-208	124	24	,	,	PUNCT
eurjchem-208	124	25	10h	10h	NUM
eurjchem-208	124	26	,	,	PUNCT
eurjchem-208	124	27	ph−h	ph−h	NOUN
eurjchem-208	124	28	)	)	PUNCT
eurjchem-208	124	29	,	,	PUNCT
eurjchem-208	124	30	8.92	8.92	NUM
eurjchem-208	124	31	(	(	PUNCT
eurjchem-208	124	32	s	s	PROPN
eurjchem-208	124	33	,	,	PUNCT
eurjchem-208	124	34	2h	2h	NUM
eurjchem-208	124	35	,	,	PUNCT
eurjchem-208	124	36	c5	c5	PROPN
eurjchem-208	124	37	–	–	PUNCT
eurjchem-208	124	38	hpyrazole	hpyrazole	NOUN
eurjchem-208	124	39	)	)	PUNCT
eurjchem-208	124	40	,	,	PUNCT
eurjchem-208	124	41	12.14	12.14	NUM
eurjchem-208	124	42	(	(	PUNCT
eurjchem-208	124	43	s	s	PROPN
eurjchem-208	124	44	,	,	PUNCT
eurjchem-208	124	45	2h	2h	NUM
eurjchem-208	124	46	,	,	PUNCT
eurjchem-208	124	47	cooh	cooh	NOUN
eurjchem-208	124	48	)	)	PUNCT
eurjchem-208	124	49	.	.	PUNCT
eurjchem-208	125	1	anal	anal	PROPN
eurjchem-208	125	2	.	.	PUNCT
eurjchem-208	125	3	calcd	calcd	NOUN
eurjchem-208	125	4	.	.	PUNCT
eurjchem-208	126	1	for	for	ADP
eurjchem-208	126	2	c20h15n4o5p	c20h15n4o5p	NUM
eurjchem-208	126	3	(	(	PUNCT
eurjchem-208	126	4	422.34	422.34	NUM
eurjchem-208	126	5	):	):	PUNCT
eurjchem-208	126	6	c	c	X
eurjchem-208	126	7	,	,	PUNCT
eurjchem-208	126	8	56.88	56.88	NUM
eurjchem-208	126	9	;	;	PUNCT
eurjchem-208	126	10	h	h	NOUN
eurjchem-208	126	11	,	,	PUNCT
eurjchem-208	126	12	3.58	3.58	NUM
eurjchem-208	126	13	;	;	PUNCT
eurjchem-208	126	14	n	n	CCONJ
eurjchem-208	126	15	,	,	PUNCT
eurjchem-208	126	16	13.27	13.27	NUM
eurjchem-208	126	17	.	.	PUNCT
eurjchem-208	126	18	found	find	VERB
eurjchem-208	126	19	:	:	PUNCT
eurjchem-208	127	1	c	c	X
eurjchem-208	127	2	,	,	PUNCT
eurjchem-208	127	3	56.61	56.61	NUM
eurjchem-208	127	4	;	;	PUNCT
eurjchem-208	128	1	h	h	NOUN
eurjchem-208	128	2	,	,	PUNCT
eurjchem-208	128	3	3.43	3.43	NUM
eurjchem-208	128	4	;	;	PUNCT
eurjchem-208	128	5	n	n	CCONJ
eurjchem-208	128	6	,	,	PUNCT
eurjchem-208	128	7	12.97	12.97	NUM
eurjchem-208	128	8	%	%	NOUN
eurjchem-208	128	9	.	.	PUNCT
eurjchem-208	129	1	2.2.4.2	2.2.4.2	NUM
eurjchem-208	129	2	.	.	PUNCT
eurjchem-208	129	3	bis{3‐(4`‐biphenyl)‐4‐carboxy‐1h‐pyrazol‐1‐yl	bis{3‐(4`‐biphenyl)‐4‐carboxy‐1h‐pyrazol‐1‐yl	ADJ
eurjchem-208	129	4	}	}	PUNCT
eurjchem-208	129	5	phosphine	phosphine	NOUN
eurjchem-208	129	6	oxide	oxide	NOUN
eurjchem-208	129	7	(	(	PUNCT
eurjchem-208	129	8	5b	5b	NUM
eurjchem-208	129	9	)	)	PUNCT
eurjchem-208	129	10	beige	beige	ADJ
eurjchem-208	129	11	crystals	crystal	NOUN
eurjchem-208	129	12	from	from	ADP
eurjchem-208	129	13	ethanol	ethanol	NOUN
eurjchem-208	129	14	in	in	ADP
eurjchem-208	129	15	77	77	NUM
eurjchem-208	129	16	%	%	NOUN
eurjchem-208	129	17	yield	yield	NOUN
eurjchem-208	129	18	.	.	PUNCT
eurjchem-208	130	1	m.p	m.p	PROPN
eurjchem-208	130	2	.	.	PROPN
eurjchem-208	130	3	:	:	PUNCT
eurjchem-208	131	1	>	>	PUNCT
eurjchem-208	131	2	300	300	NUM
eurjchem-208	131	3	°	°	NOUN
eurjchem-208	131	4	c	c	NOUN
eurjchem-208	131	5	.	.	PUNCT
eurjchem-208	132	1	ir	ir	PROPN
eurjchem-208	132	2	(	(	PUNCT
eurjchem-208	132	3	kbr	kbr	PROPN
eurjchem-208	132	4	,	,	PUNCT
eurjchem-208	132	5	max	max	PROPN
eurjchem-208	132	6	,	,	PUNCT
eurjchem-208	132	7	cm‐1	cm‐1	PROPN
eurjchem-208	132	8	):	):	PUNCT
eurjchem-208	132	9	3243	3243	NUM
eurjchem-208	132	10	(	(	PUNCT
eurjchem-208	132	11	br	br	PROPN
eurjchem-208	132	12	,	,	PUNCT
eurjchem-208	132	13	oh	oh	INTJ
eurjchem-208	132	14	)	)	PUNCT
eurjchem-208	132	15	,	,	PUNCT
eurjchem-208	132	16	2360	2360	NUM
eurjchem-208	132	17	(	(	PUNCT
eurjchem-208	132	18	p	p	X
eurjchem-208	132	19	–	–	PUNCT
eurjchem-208	132	20	h	h	NOUN
eurjchem-208	132	21	)	)	PUNCT
eurjchem-208	132	22	,	,	PUNCT
eurjchem-208	132	23	1711	1711	NUM
eurjchem-208	132	24	(	(	PUNCT
eurjchem-208	132	25	c	c	NOUN
eurjchem-208	132	26	=	=	NOUN
eurjchem-208	132	27	o	o	NOUN
eurjchem-208	132	28	)	)	PUNCT
eurjchem-208	132	29	,	,	PUNCT
eurjchem-208	132	30	1239	1239	NUM
eurjchem-208	132	31	(	(	PUNCT
eurjchem-208	132	32	p	p	NOUN
eurjchem-208	132	33	=	=	NOUN
eurjchem-208	132	34	o	o	NOUN
eurjchem-208	132	35	)	)	PUNCT
eurjchem-208	132	36	.	.	PUNCT
eurjchem-208	133	1	1h	1h	NUM
eurjchem-208	133	2	nmr	nmr	NOUN
eurjchem-208	133	3	(	(	PUNCT
eurjchem-208	133	4	dmso	dmso	NOUN
eurjchem-208	133	5	,	,	PUNCT
eurjchem-208	133	6	δ	δ	PROPN
eurjchem-208	133	7	ppm	ppm	VERB
eurjchem-208	133	8	):	):	PUNCT
eurjchem-208	133	9	7.32	7.32	NUM
eurjchem-208	133	10	(	(	PUNCT
eurjchem-208	133	11	d	d	PROPN
eurjchem-208	133	12	,	,	PUNCT
eurjchem-208	133	13	1h	1h	NUM
eurjchem-208	133	14	,	,	PUNCT
eurjchem-208	133	15	jph=468	jph=468	NOUN
eurjchem-208	133	16	hz	hz	VERB
eurjchem-208	133	17	,	,	PUNCT
eurjchem-208	133	18	p	p	NOUN
eurjchem-208	133	19	–	–	PUNCT
eurjchem-208	133	20	h	h	NOUN
eurjchem-208	133	21	)	)	PUNCT
eurjchem-208	133	22	,	,	PUNCT
eurjchem-208	133	23	6.67–7.82	6.67–7.82	NUM
eurjchem-208	133	24	(	(	PUNCT
eurjchem-208	133	25	m	m	PROPN
eurjchem-208	133	26	,	,	PUNCT
eurjchem-208	133	27	18h	18h	NOUN
eurjchem-208	133	28	,	,	PUNCT
eurjchem-208	133	29	ar−h	ar−h	NOUN
eurjchem-208	133	30	)	)	PUNCT
eurjchem-208	133	31	,	,	PUNCT
eurjchem-208	133	32	8.13	8.13	NUM
eurjchem-208	133	33	(	(	PUNCT
eurjchem-208	133	34	s	s	PROPN
eurjchem-208	133	35	,	,	PUNCT
eurjchem-208	133	36	2h	2h	NUM
eurjchem-208	133	37	,	,	PUNCT
eurjchem-208	133	38	c5	c5	PROPN
eurjchem-208	133	39	–	–	PUNCT
eurjchem-208	133	40	hpyrazole	hpyrazole	NOUN
eurjchem-208	133	41	)	)	PUNCT
eurjchem-208	133	42	,	,	PUNCT
eurjchem-208	133	43	11.80	11.80	NUM
eurjchem-208	133	44	(	(	PUNCT
eurjchem-208	133	45	s	s	PROPN
eurjchem-208	133	46	,	,	PUNCT
eurjchem-208	133	47	2h	2h	NUM
eurjchem-208	133	48	,	,	PUNCT
eurjchem-208	133	49	cooh	cooh	NOUN
eurjchem-208	133	50	)	)	PUNCT
eurjchem-208	133	51	.	.	PUNCT
eurjchem-208	134	1	anal	anal	PROPN
eurjchem-208	134	2	.	.	PUNCT
eurjchem-208	134	3	calcd	calcd	NOUN
eurjchem-208	134	4	.	.	PUNCT
eurjchem-208	135	1	for	for	SCONJ
eurjchem-208	135	2	c32h23n4o5p	c32h23n4o5p	PROPN
eurjchem-208	135	3	(	(	PUNCT
eurjchem-208	135	4	574.54	574.54	NUM
eurjchem-208	135	5	):	):	PUNCT
eurjchem-208	135	6	c	c	NOUN
eurjchem-208	135	7	,	,	PUNCT
eurjchem-208	135	8	66.90	66.90	NUM
eurjchem-208	135	9	;	;	PUNCT
eurjchem-208	135	10	h	h	NOUN
eurjchem-208	135	11	,	,	PUNCT
eurjchem-208	135	12	4.04	4.04	NUM
eurjchem-208	135	13	;	;	PUNCT
eurjchem-208	135	14	n	n	CCONJ
eurjchem-208	135	15	,	,	PUNCT
eurjchem-208	135	16	9.75	9.75	NUM
eurjchem-208	135	17	.	.	PUNCT
eurjchem-208	135	18	found	find	VERB
eurjchem-208	135	19	:	:	PUNCT
eurjchem-208	136	1	c	c	X
eurjchem-208	136	2	,	,	PUNCT
eurjchem-208	136	3	66.61	66.61	NUM
eurjchem-208	136	4	;	;	PUNCT
eurjchem-208	136	5	h	h	NOUN
eurjchem-208	136	6	,	,	PUNCT
eurjchem-208	136	7	3.87	3.87	NUM
eurjchem-208	136	8	;	;	PUNCT
eurjchem-208	136	9	n	n	CCONJ
eurjchem-208	136	10	,	,	PUNCT
eurjchem-208	136	11	9.52	9.52	NUM
eurjchem-208	136	12	%	%	NOUN
eurjchem-208	136	13	.	.	PUNCT
eurjchem-208	137	1	2.2.5	2.2.5	X
eurjchem-208	137	2	.	.	PUNCT
eurjchem-208	137	3	bis{chromeno[4,3‐c]pyrazol‐4‐oxo‐2‐yl}phosphine	bis{chromeno[4,3‐c]pyrazol‐4‐oxo‐2‐yl}phosphine	PROPN
eurjchem-208	137	4	oxide	oxide	NOUN
eurjchem-208	137	5	(	(	PUNCT
eurjchem-208	137	6	7	7	NUM
eurjchem-208	137	7	)	)	PUNCT
eurjchem-208	137	8	a	a	DET
eurjchem-208	137	9	mixture	mixture	NOUN
eurjchem-208	137	10	of	of	ADP
eurjchem-208	137	11	6	6	NUM
eurjchem-208	137	12	(	(	PUNCT
eurjchem-208	137	13	0.001	0.001	NUM
eurjchem-208	137	14	mol	mol	NOUN
eurjchem-208	137	15	,	,	PUNCT
eurjchem-208	137	16	0.422	0.422	NUM
eurjchem-208	137	17	g)and	g)and	NOUN
eurjchem-208	137	18	selenium	selenium	NOUN
eurjchem-208	137	19	dioxide	dioxide	NOUN
eurjchem-208	137	20	(	(	PUNCT
eurjchem-208	137	21	0.002	0.002	NUM
eurjchem-208	137	22	mol	mol	NOUN
eurjchem-208	137	23	,	,	PUNCT
eurjchem-208	137	24	0.22	0.22	NUM
eurjchem-208	137	25	g	g	NOUN
eurjchem-208	137	26	)	)	PUNCT
eurjchem-208	137	27	in	in	ADP
eurjchem-208	137	28	dry	dry	ADJ
eurjchem-208	137	29	dioxane	dioxane	NOUN
eurjchem-208	137	30	(	(	PUNCT
eurjchem-208	137	31	15	15	NUM
eurjchem-208	137	32	cm3	cm3	NOUN
eurjchem-208	137	33	)	)	PUNCT
eurjchem-208	137	34	was	be	AUX
eurjchem-208	137	35	refluxed	refluxe	VERB
eurjchem-208	137	36	for	for	ADP
eurjchem-208	137	37	5	5	NUM
eurjchem-208	137	38	h.	h.	NOUN
eurjchem-208	137	39	the	the	DET
eurjchem-208	137	40	reaction	reaction	NOUN
eurjchem-208	137	41	mixture	mixture	NOUN
eurjchem-208	137	42	was	be	AUX
eurjchem-208	137	43	filtered	filter	VERB
eurjchem-208	137	44	off	off	ADP
eurjchem-208	137	45	while	while	SCONJ
eurjchem-208	137	46	hot	hot	ADJ
eurjchem-208	137	47	.	.	PUNCT
eurjchem-208	138	1	some	some	DET
eurjchem-208	138	2	water	water	NOUN
eurjchem-208	138	3	(	(	PUNCT
eurjchem-208	138	4	20	20	NUM
eurjchem-208	138	5	cm3	cm3	NOUN
eurjchem-208	138	6	)	)	PUNCT
eurjchem-208	138	7	was	be	AUX
eurjchem-208	138	8	added	add	VERB
eurjchem-208	138	9	to	to	ADP
eurjchem-208	138	10	the	the	DET
eurjchem-208	138	11	filtrate	filtrate	NOUN
eurjchem-208	138	12	,	,	PUNCT
eurjchem-208	138	13	and	and	CCONJ
eurjchem-208	138	14	then	then	ADV
eurjchem-208	138	15	left	leave	VERB
eurjchem-208	138	16	for	for	ADP
eurjchem-208	138	17	complete	complete	ADJ
eurjchem-208	138	18	precipitation	precipitation	NOUN
eurjchem-208	138	19	.	.	PUNCT
eurjchem-208	139	1	the	the	DET
eurjchem-208	139	2	resulting	result	VERB
eurjchem-208	139	3	precipitate	precipitate	NOUN
eurjchem-208	139	4	was	be	AUX
eurjchem-208	139	5	filtered	filter	VERB
eurjchem-208	139	6	off	off	ADP
eurjchem-208	139	7	and	and	CCONJ
eurjchem-208	139	8	crystallized	crystallize	VERB
eurjchem-208	139	9	from	from	ADP
eurjchem-208	139	10	dilute	dilute	ADJ
eurjchem-208	139	11	dimethylformamide	dimethylformamide	NOUN
eurjchem-208	139	12	to	to	PART
eurjchem-208	139	13	give	give	VERB
eurjchem-208	139	14	deep	deep	ADJ
eurjchem-208	139	15	red	red	ADJ
eurjchem-208	139	16	crystals	crystal	NOUN
eurjchem-208	139	17	in	in	ADP
eurjchem-208	139	18	75	75	NUM
eurjchem-208	139	19	%	%	NOUN
eurjchem-208	139	20	yield	yield	NOUN
eurjchem-208	139	21	.	.	PUNCT
eurjchem-208	140	1	m.p	m.p	PROPN
eurjchem-208	140	2	.	.	PROPN
eurjchem-208	140	3	:	:	PUNCT
eurjchem-208	141	1	>	>	PUNCT
eurjchem-208	141	2	300	300	NUM
eurjchem-208	141	3	°	°	NOUN
eurjchem-208	141	4	c	c	NOUN
eurjchem-208	141	5	.	.	PUNCT
eurjchem-208	142	1	ir	ir	PROPN
eurjchem-208	142	2	(	(	PUNCT
eurjchem-208	142	3	kbr	kbr	PROPN
eurjchem-208	142	4	,	,	PUNCT
eurjchem-208	142	5	max	max	PROPN
eurjchem-208	142	6	,	,	PUNCT
eurjchem-208	142	7	cm‐1	cm‐1	PROPN
eurjchem-208	142	8	):	):	PUNCT
eurjchem-208	142	9	3054	3054	NUM
eurjchem-208	142	10	(	(	PUNCT
eurjchem-208	142	11	c	c	X
eurjchem-208	142	12	–	–	PUNCT
eurjchem-208	142	13	harom	harom	NOUN
eurjchem-208	142	14	)	)	PUNCT
eurjchem-208	142	15	,	,	PUNCT
eurjchem-208	142	16	2360	2360	NUM
eurjchem-208	142	17	(	(	PUNCT
eurjchem-208	142	18	p	p	X
eurjchem-208	142	19	–	–	PUNCT
eurjchem-208	142	20	h	h	NOUN
eurjchem-208	142	21	)	)	PUNCT
eurjchem-208	142	22	,	,	PUNCT
eurjchem-208	142	23	1652	1652	NUM
eurjchem-208	142	24	(	(	PUNCT
eurjchem-208	142	25	c	c	NOUN
eurjchem-208	142	26	=	=	NOUN
eurjchem-208	142	27	o	o	NOUN
eurjchem-208	142	28	)	)	PUNCT
eurjchem-208	142	29	,	,	PUNCT
eurjchem-208	142	30	1624	1624	NUM
eurjchem-208	142	31	(	(	PUNCT
eurjchem-208	142	32	c	c	NOUN
eurjchem-208	142	33	=	=	SYM
eurjchem-208	142	34	n	n	NUM
eurjchem-208	142	35	)	)	PUNCT
eurjchem-208	142	36	,	,	PUNCT
eurjchem-208	142	37	1592	1592	NUM
eurjchem-208	142	38	(	(	PUNCT
eurjchem-208	142	39	c	c	X
eurjchem-208	142	40	=	=	SYM
eurjchem-208	142	41	c	c	NOUN
eurjchem-208	142	42	)	)	PUNCT
eurjchem-208	142	43	,	,	PUNCT
eurjchem-208	142	44	1277	1277	NUM
eurjchem-208	142	45	(	(	PUNCT
eurjchem-208	142	46	p	p	NOUN
eurjchem-208	142	47	=	=	NOUN
eurjchem-208	142	48	o	o	NOUN
eurjchem-208	142	49	)	)	PUNCT
eurjchem-208	142	50	,	,	PUNCT
eurjchem-208	142	51	1080	1080	NUM
eurjchem-208	142	52	(	(	PUNCT
eurjchem-208	142	53	c	c	NOUN
eurjchem-208	142	54	–	–	PUNCT
eurjchem-208	142	55	o	o	NOUN
eurjchem-208	142	56	–	–	PUNCT
eurjchem-208	142	57	c	c	NOUN
eurjchem-208	142	58	)	)	PUNCT
eurjchem-208	142	59	.	.	PUNCT
eurjchem-208	143	1	1h	1h	NUM
eurjchem-208	143	2	nmr	nmr	NOUN
eurjchem-208	143	3	(	(	PUNCT
eurjchem-208	143	4	dmso	dmso	NOUN
eurjchem-208	143	5	,	,	PUNCT
eurjchem-208	143	6	δ	δ	PROPN
eurjchem-208	143	7	ppm	ppm	VERB
eurjchem-208	143	8	):	):	PUNCT
eurjchem-208	143	9	7.21	7.21	NUM
eurjchem-208	143	10	(	(	PUNCT
eurjchem-208	143	11	d	d	PROPN
eurjchem-208	143	12	,	,	PUNCT
eurjchem-208	143	13	1h	1h	NUM
eurjchem-208	143	14	,	,	PUNCT
eurjchem-208	143	15	jph=425	jph=425	PROPN
eurjchem-208	143	16	hz	hz	PROPN
eurjchem-208	143	17	,	,	PUNCT
eurjchem-208	143	18	p	p	NOUN
eurjchem-208	143	19	–	–	PUNCT
eurjchem-208	143	20	h	h	NOUN
eurjchem-208	143	21	)	)	PUNCT
eurjchem-208	143	22	,	,	PUNCT
eurjchem-208	143	23	7.32	7.32	NUM
eurjchem-208	143	24	(	(	PUNCT
eurjchem-208	143	25	t	t	PROPN
eurjchem-208	143	26	,	,	PUNCT
eurjchem-208	143	27	2h	2h	NUM
eurjchem-208	143	28	,	,	PUNCT
eurjchem-208	143	29	j=8.8	j=8.8	PROPN
eurjchem-208	143	30	hz	hz	PROPN
eurjchem-208	143	31	,	,	PUNCT
eurjchem-208	143	32	ar	ar	PROPN
eurjchem-208	143	33	–	–	PROPN
eurjchem-208	143	34	h	h	NOUN
eurjchem-208	143	35	)	)	PUNCT
eurjchem-208	143	36	,	,	PUNCT
eurjchem-208	143	37	7.46	7.46	NUM
eurjchem-208	143	38	(	(	PUNCT
eurjchem-208	143	39	t	t	PROPN
eurjchem-208	143	40	,	,	PUNCT
eurjchem-208	143	41	2h	2h	NUM
eurjchem-208	143	42	,	,	PUNCT
eurjchem-208	143	43	j=8.0	j=8.0	PROPN
eurjchem-208	143	44	hz	hz	PROPN
eurjchem-208	143	45	,	,	PUNCT
eurjchem-208	143	46	ar	ar	PROPN
eurjchem-208	143	47	–	–	PROPN
eurjchem-208	143	48	h	h	NOUN
eurjchem-208	143	49	)	)	PUNCT
eurjchem-208	143	50	,	,	PUNCT
eurjchem-208	143	51	7.58	7.58	NUM
eurjchem-208	143	52	(	(	PUNCT
eurjchem-208	143	53	d	d	PROPN
eurjchem-208	143	54	,	,	PUNCT
eurjchem-208	143	55	2h	2h	NUM
eurjchem-208	143	56	,	,	PUNCT
eurjchem-208	143	57	j=8.2	j=8.2	NOUN
eurjchem-208	143	58	hz	hz	NOUN
eurjchem-208	143	59	,	,	PUNCT
eurjchem-208	143	60	ar	ar	PROPN
eurjchem-208	143	61	–	–	PROPN
eurjchem-208	143	62	h	h	NOUN
eurjchem-208	143	63	)	)	PUNCT
eurjchem-208	143	64	,	,	PUNCT
eurjchem-208	143	65	7.94	7.94	NUM
eurjchem-208	143	66	(	(	PUNCT
eurjchem-208	143	67	d	d	PROPN
eurjchem-208	143	68	,	,	PUNCT
eurjchem-208	143	69	2h	2h	NUM
eurjchem-208	143	70	,	,	PUNCT
eurjchem-208	143	71	j=7.8	j=7.8	NOUN
eurjchem-208	143	72	hz	hz	NOUN
eurjchem-208	143	73	,	,	PUNCT
eurjchem-208	143	74	ar	ar	PROPN
eurjchem-208	143	75	–	–	PUNCT
eurjchem-208	143	76	h),8.64	h),8.64	PROPN
eurjchem-208	143	77	(	(	PUNCT
eurjchem-208	143	78	s	s	PROPN
eurjchem-208	143	79	,	,	PUNCT
eurjchem-208	143	80	2h	2h	NUM
eurjchem-208	143	81	,	,	PUNCT
eurjchem-208	143	82	c5	c5	PROPN
eurjchem-208	143	83	–	–	PUNCT
eurjchem-208	143	84	hpyrazole	hpyrazole	NOUN
eurjchem-208	143	85	)	)	PUNCT
eurjchem-208	143	86	.	.	PUNCT
eurjchem-208	144	1	anal	anal	PROPN
eurjchem-208	144	2	.	.	PUNCT
eurjchem-208	144	3	calcd	calcd	NOUN
eurjchem-208	144	4	.	.	PUNCT
eurjchem-208	145	1	for	for	ADP
eurjchem-208	145	2	c20h11n4o5p	c20h11n4o5p	PROPN
eurjchem-208	145	3	(	(	PUNCT
eurjchem-208	145	4	418.31	418.31	NUM
eurjchem-208	145	5	):	):	PUNCT
eurjchem-208	145	6	c	c	X
eurjchem-208	145	7	,	,	PUNCT
eurjchem-208	145	8	57.43	57.43	NUM
eurjchem-208	145	9	;	;	PUNCT
eurjchem-208	145	10	h	h	NOUN
eurjchem-208	145	11	,	,	PUNCT
eurjchem-208	145	12	2.65	2.65	NUM
eurjchem-208	145	13	;	;	PUNCT
eurjchem-208	145	14	n	n	CCONJ
eurjchem-208	145	15	,	,	PUNCT
eurjchem-208	145	16	13.39	13.39	NUM
eurjchem-208	145	17	.	.	PUNCT
eurjchem-208	145	18	found	find	VERB
eurjchem-208	145	19	:	:	PUNCT
eurjchem-208	146	1	c	c	X
eurjchem-208	146	2	,	,	PUNCT
eurjchem-208	146	3	57.09	57.09	NUM
eurjchem-208	146	4	;	;	PUNCT
eurjchem-208	146	5	h	h	NOUN
eurjchem-208	146	6	,	,	PUNCT
eurjchem-208	146	7	2.43	2.43	NUM
eurjchem-208	146	8	;	;	PUNCT
eurjchem-208	146	9	n	n	CCONJ
eurjchem-208	146	10	,	,	PUNCT
eurjchem-208	146	11	13.04	13.04	NUM
eurjchem-208	146	12	%	%	NOUN
eurjchem-208	146	13	.	.	PUNCT
eurjchem-208	147	1	2.2.6	2.2.6	X
eurjchem-208	147	2	.	.	PUNCT
eurjchem-208	147	3	bis{3‐phenyl‐4‐[(phenylimino)methyl]‐1h‐pyrazol‐1‐	bis{3‐phenyl‐4‐[(phenylimino)methyl]‐1h‐pyrazol‐1‐	VERB
eurjchem-208	147	4	yl}phosphine	yl}phosphine	PRON
eurjchem-208	147	5	oxide(9	oxide(9	PROPN
eurjchem-208	147	6	)	)	PUNCT
eurjchem-208	147	7	a	a	DET
eurjchem-208	147	8	mixture	mixture	NOUN
eurjchem-208	147	9	of	of	ADP
eurjchem-208	147	10	bis‐(4‐formylpyrazolyl)phosphine	bis‐(4‐formylpyrazolyl)phosphine	NOUN
eurjchem-208	147	11	oxide	oxide	NOUN
eurjchem-208	147	12	4a	4a	X
eurjchem-208	147	13	(	(	PUNCT
eurjchem-208	147	14	0.001	0.001	NUM
eurjchem-208	147	15	mol	mol	NOUN
eurjchem-208	147	16	,	,	PUNCT
eurjchem-208	147	17	0.39	0.39	NUM
eurjchem-208	147	18	g	g	NOUN
eurjchem-208	147	19	)	)	PUNCT
eurjchem-208	147	20	and	and	CCONJ
eurjchem-208	147	21	freshly	freshly	ADV
eurjchem-208	147	22	distillated	distillate	VERB
eurjchem-208	147	23	aniline	aniline	NOUN
eurjchem-208	147	24	(	(	PUNCT
eurjchem-208	147	25	0.002	0.002	NUM
eurjchem-208	147	26	mol	mol	NOUN
eurjchem-208	147	27	,	,	PUNCT
eurjchem-208	147	28	0.186	0.186	NUM
eurjchem-208	147	29	g	g	NOUN
eurjchem-208	147	30	)	)	PUNCT
eurjchem-208	147	31	in	in	ADP
eurjchem-208	147	32	absolute	absolute	ADJ
eurjchem-208	147	33	ethanol	ethanol	NOUN
eurjchem-208	147	34	(	(	PUNCT
eurjchem-208	147	35	10	10	NUM
eurjchem-208	147	36	cm3	cm3	NOUN
eurjchem-208	147	37	)	)	PUNCT
eurjchem-208	147	38	was	be	AUX
eurjchem-208	147	39	refluxed	refluxe	VERB
eurjchem-208	147	40	for	for	ADP
eurjchem-208	147	41	4	4	NUM
eurjchem-208	147	42	h.	h.	NOUN
eurjchem-208	147	43	the	the	DET
eurjchem-208	147	44	solvent	solvent	NOUN
eurjchem-208	147	45	was	be	AUX
eurjchem-208	147	46	concentrated	concentrate	VERB
eurjchem-208	147	47	to	to	ADP
eurjchem-208	147	48	half	half	DET
eurjchem-208	147	49	its	its	PRON
eurjchem-208	147	50	volume	volume	NOUN
eurjchem-208	147	51	and	and	CCONJ
eurjchem-208	147	52	left	leave	VERB
eurjchem-208	147	53	for	for	ADP
eurjchem-208	147	54	two	two	NUM
eurjchem-208	147	55	days	day	NOUN
eurjchem-208	147	56	for	for	ADP
eurjchem-208	147	57	complete	complete	ADJ
eurjchem-208	147	58	precipitation	precipitation	NOUN
eurjchem-208	147	59	.	.	PUNCT
eurjchem-208	148	1	the	the	DET
eurjchem-208	148	2	formed	form	VERB
eurjchem-208	148	3	solid	solid	NOUN
eurjchem-208	148	4	was	be	AUX
eurjchem-208	148	5	filtered	filter	VERB
eurjchem-208	148	6	off	off	ADP
eurjchem-208	148	7	and	and	CCONJ
eurjchem-208	148	8	crystallized	crystallize	VERB
eurjchem-208	148	9	from	from	ADP
eurjchem-208	148	10	dilute	dilute	NOUN
eurjchem-208	148	11	ethanol	ethanol	NOUN
eurjchem-208	148	12	to	to	PART
eurjchem-208	148	13	give	give	VERB
eurjchem-208	148	14	yellow	yellow	ADJ
eurjchem-208	148	15	crystals	crystal	NOUN
eurjchem-208	148	16	in	in	ADP
eurjchem-208	148	17	66	66	NUM
eurjchem-208	148	18	%	%	NOUN
eurjchem-208	148	19	yield	yield	NOUN
eurjchem-208	148	20	.	.	PUNCT
eurjchem-208	149	1	m.p	m.p	PROPN
eurjchem-208	149	2	.	.	PROPN
eurjchem-208	149	3	:	:	PUNCT
eurjchem-208	150	1	148‐150	148‐150	PROPN
eurjchem-208	150	2	°	°	SYM
eurjchem-208	150	3	c	c	X
eurjchem-208	150	4	.	.	PUNCT
eurjchem-208	151	1	ir	ir	PROPN
eurjchem-208	151	2	(	(	PUNCT
eurjchem-208	151	3	kbr	kbr	PROPN
eurjchem-208	151	4	,	,	PUNCT
eurjchem-208	151	5	max	max	PROPN
eurjchem-208	151	6	,	,	PUNCT
eurjchem-208	151	7	cm‐1	cm‐1	PROPN
eurjchem-208	151	8	):	):	PUNCT
eurjchem-208	151	9	3050	3050	NUM
eurjchem-208	151	10	(	(	PUNCT
eurjchem-208	151	11	c	c	X
eurjchem-208	151	12	–	–	PUNCT
eurjchem-208	151	13	harom	harom	NOUN
eurjchem-208	151	14	)	)	PUNCT
eurjchem-208	151	15	,	,	PUNCT
eurjchem-208	151	16	2498	2498	NUM
eurjchem-208	151	17	(	(	PUNCT
eurjchem-208	151	18	p	p	NOUN
eurjchem-208	151	19	–	–	PUNCT
eurjchem-208	151	20	h	h	NOUN
eurjchem-208	151	21	)	)	PUNCT
eurjchem-208	151	22	,	,	PUNCT
eurjchem-208	151	23	1631	1631	NUM
eurjchem-208	151	24	(	(	PUNCT
eurjchem-208	151	25	c	c	NOUN
eurjchem-208	151	26	=	=	NOUN
eurjchem-208	151	27	nexocyclic	nexocyclic	ADJ
eurjchem-208	151	28	)	)	PUNCT
eurjchem-208	151	29	,	,	PUNCT
eurjchem-208	151	30	1540	1540	NUM
eurjchem-208	151	31	(	(	PUNCT
eurjchem-208	151	32	c	c	X
eurjchem-208	151	33	=	=	SYM
eurjchem-208	151	34	c	c	NOUN
eurjchem-208	151	35	)	)	PUNCT
eurjchem-208	151	36	,	,	PUNCT
eurjchem-208	151	37	1230	1230	NUM
eurjchem-208	151	38	(	(	PUNCT
eurjchem-208	151	39	p	p	NOUN
eurjchem-208	151	40	=	=	NOUN
eurjchem-208	151	41	o	o	NOUN
eurjchem-208	151	42	)	)	PUNCT
eurjchem-208	151	43	.	.	PUNCT
eurjchem-208	152	1	1h	1h	NUM
eurjchem-208	152	2	nmr	nmr	NOUN
eurjchem-208	152	3	(	(	PUNCT
eurjchem-208	152	4	dmso	dmso	NOUN
eurjchem-208	152	5	,	,	PUNCT
eurjchem-208	152	6	δ	δ	PROPN
eurjchem-208	152	7	ppm	ppm	VERB
eurjchem-208	152	8	):	):	PUNCT
eurjchem-208	152	9	7.69	7.69	NUM
eurjchem-208	152	10	(	(	PUNCT
eurjchem-208	152	11	d	d	PROPN
eurjchem-208	152	12	,	,	PUNCT
eurjchem-208	152	13	1h	1h	NUM
eurjchem-208	152	14	,	,	PUNCT
eurjchem-208	152	15	jph=608	jph=608	PROPN
eurjchem-208	152	16	hz	hz	VERB
eurjchem-208	152	17	,	,	PUNCT
eurjchem-208	152	18	p	p	NOUN
eurjchem-208	152	19	–	–	PUNCT
eurjchem-208	152	20	h	h	NOUN
eurjchem-208	152	21	)	)	PUNCT
eurjchem-208	152	22	,	,	PUNCT
eurjchem-208	152	23	7.11	7.11	NUM
eurjchem-208	152	24	–	–	PUNCT
eurjchem-208	152	25	8.10	8.10	NUM
eurjchem-208	152	26	(	(	PUNCT
eurjchem-208	152	27	m	m	PROPN
eurjchem-208	152	28	,	,	PUNCT
eurjchem-208	152	29	20h	20h	NOUN
eurjchem-208	152	30	,	,	PUNCT
eurjchem-208	152	31	ph−h	ph−h	NOUN
eurjchem-208	152	32	)	)	PUNCT
eurjchem-208	152	33	,	,	PUNCT
eurjchem-208	152	34	8.56	8.56	NUM
eurjchem-208	152	35	(	(	PUNCT
eurjchem-208	152	36	s	s	PROPN
eurjchem-208	152	37	,	,	PUNCT
eurjchem-208	152	38	2h	2h	NUM
eurjchem-208	152	39	,	,	PUNCT
eurjchem-208	152	40	c5	c5	PROPN
eurjchem-208	152	41	–	–	PUNCT
eurjchem-208	152	42	hpyrazole	hpyrazole	NOUN
eurjchem-208	152	43	)	)	PUNCT
eurjchem-208	152	44	,	,	PUNCT
eurjchem-208	152	45	9.36	9.36	NUM
eurjchem-208	152	46	(	(	PUNCT
eurjchem-208	152	47	s	s	PROPN
eurjchem-208	152	48	,	,	PUNCT
eurjchem-208	152	49	2h	2h	NUM
eurjchem-208	152	50	,	,	PUNCT
eurjchem-208	152	51	ch	ch	NOUN
eurjchem-208	152	52	=	=	NOUN
eurjchem-208	152	53	nexocyclic	nexocyclic	ADJ
eurjchem-208	152	54	)	)	PUNCT
eurjchem-208	152	55	.	.	PUNCT
eurjchem-208	153	1	ms	ms	NOUN
eurjchem-208	153	2	(	(	PUNCT
eurjchem-208	153	3	m	m	PROPN
eurjchem-208	153	4	/	/	SYM
eurjchem-208	153	5	e	e	NOUN
eurjchem-208	153	6	,	,	PUNCT
eurjchem-208	153	7	%	%	INTJ
eurjchem-208	153	8	):	):	PUNCT
eurjchem-208	153	9	520	520	NUM
eurjchem-208	153	10	(	(	PUNCT
eurjchem-208	153	11	m+–h2o,–h2	m+–h2o,–h2	PROPN
eurjchem-208	153	12	,	,	PUNCT
eurjchem-208	153	13	1	1	NUM
eurjchem-208	153	14	%	%	NOUN
eurjchem-208	153	15	)	)	PUNCT
eurjchem-208	153	16	,	,	PUNCT
eurjchem-208	153	17	423	423	NUM
eurjchem-208	153	18	(	(	PUNCT
eurjchem-208	153	19	1	1	NUM
eurjchem-208	153	20	)	)	PUNCT
eurjchem-208	153	21	,	,	PUNCT
eurjchem-208	153	22	260	260	NUM
eurjchem-208	153	23	(	(	PUNCT
eurjchem-208	153	24	42	42	NUM
eurjchem-208	153	25	)	)	PUNCT
eurjchem-208	153	26	,	,	PUNCT
eurjchem-208	153	27	246	246	NUM
eurjchem-208	153	28	(	(	PUNCT
eurjchem-208	153	29	24	24	NUM
eurjchem-208	153	30	)	)	PUNCT
eurjchem-208	153	31	,	,	PUNCT
eurjchem-208	153	32	130	130	NUM
eurjchem-208	153	33	(	(	PUNCT
eurjchem-208	153	34	12	12	NUM
eurjchem-208	153	35	)	)	PUNCT
eurjchem-208	153	36	,	,	PUNCT
eurjchem-208	153	37	77	77	NUM
eurjchem-208	153	38	(	(	PUNCT
eurjchem-208	153	39	100	100	NUM
eurjchem-208	153	40	)	)	PUNCT
eurjchem-208	153	41	,	,	PUNCT
eurjchem-208	153	42	51	51	NUM
eurjchem-208	153	43	(	(	PUNCT
eurjchem-208	153	44	48	48	NUM
eurjchem-208	153	45	)	)	PUNCT
eurjchem-208	153	46	.	.	PUNCT
eurjchem-208	154	1	anal	anal	PROPN
eurjchem-208	154	2	.	.	PUNCT
eurjchem-208	154	3	calcd	calcd	NOUN
eurjchem-208	154	4	for	for	ADP
eurjchem-208	154	5	c32h25n4op	c32h25n4op	NOUN
eurjchem-208	154	6	(	(	PUNCT
eurjchem-208	154	7	540.57	540.57	NUM
eurjchem-208	154	8	):	):	PUNCT
eurjchem-208	154	9	c	c	NOUN
eurjchem-208	154	10	,	,	PUNCT
eurjchem-208	154	11	71.10	71.10	NUM
eurjchem-208	154	12	;	;	PUNCT
eurjchem-208	154	13	h	h	NOUN
eurjchem-208	154	14	,	,	PUNCT
eurjchem-208	154	15	4.66	4.66	NUM
eurjchem-208	154	16	;	;	PUNCT
eurjchem-208	154	17	n	n	CCONJ
eurjchem-208	154	18	,	,	PUNCT
eurjchem-208	154	19	15.55	15.55	NUM
eurjchem-208	154	20	.	.	PUNCT
eurjchem-208	154	21	found	find	VERB
eurjchem-208	154	22	:	:	PUNCT
eurjchem-208	155	1	c	c	X
eurjchem-208	155	2	,	,	PUNCT
eurjchem-208	155	3	70.83	70.83	NUM
eurjchem-208	155	4	;	;	PUNCT
eurjchem-208	155	5	h	h	NOUN
eurjchem-208	155	6	,	,	PUNCT
eurjchem-208	155	7	4.34	4.34	NUM
eurjchem-208	155	8	;	;	PUNCT
eurjchem-208	155	9	n	n	CCONJ
eurjchem-208	155	10	,	,	PUNCT
eurjchem-208	155	11	15.23	15.23	NUM
eurjchem-208	155	12	%	%	NOUN
eurjchem-208	155	13	.	.	PUNCT
eurjchem-208	156	1	2.2.7	2.2.7	X
eurjchem-208	156	2	.	.	PUNCT
eurjchem-208	157	1	bis{3‐phenyl‐4‐[3‐phenyl‐4‐oxo‐1,3‐thiazolidin‐2‐yl]‐	bis{3‐phenyl‐4‐[3‐phenyl‐4‐oxo‐1,3‐thiazolidin‐2‐yl]‐	PROPN
eurjchem-208	157	2	1h‐pyrazol‐1‐yl}phosphine	1h‐pyrazol‐1‐yl}phosphine	NUM
eurjchem-208	157	3	oxide	oxide	NOUN
eurjchem-208	157	4	(	(	PUNCT
eurjchem-208	157	5	10	10	NUM
eurjchem-208	157	6	)	)	PUNCT
eurjchem-208	157	7	method	method	NOUN
eurjchem-208	157	8	a	a	PRON
eurjchem-208	157	9	:	:	PUNCT
eurjchem-208	157	10	a	a	DET
eurjchem-208	157	11	mixture	mixture	NOUN
eurjchem-208	157	12	of	of	ADP
eurjchem-208	157	13	bis‐schiff	bis‐schiff	PROPN
eurjchem-208	157	14	's	's	PART
eurjchem-208	157	15	base	base	NOUN
eurjchem-208	157	16	9	9	NUM
eurjchem-208	157	17	(	(	PUNCT
eurjchem-208	157	18	0.001	0.001	NUM
eurjchem-208	157	19	mol	mol	NOUN
eurjchem-208	157	20	,	,	PUNCT
eurjchem-208	157	21	0.54	0.54	NUM
eurjchem-208	157	22	g	g	NOUN
eurjchem-208	157	23	)	)	PUNCT
eurjchem-208	157	24	and	and	CCONJ
eurjchem-208	157	25	thioglycolic	thioglycolic	ADJ
eurjchem-208	157	26	acid	acid	NOUN
eurjchem-208	157	27	(	(	PUNCT
eurjchem-208	157	28	0.0025	0.0025	NUM
eurjchem-208	157	29	mol	mol	NOUN
eurjchem-208	157	30	,	,	PUNCT
eurjchem-208	157	31	0.23	0.23	NUM
eurjchem-208	157	32	g	g	NOUN
eurjchem-208	157	33	)	)	PUNCT
eurjchem-208	157	34	in	in	ADP
eurjchem-208	157	35	dry	dry	ADJ
eurjchem-208	157	36	dimethylformamide	dimethylformamide	NOUN
eurjchem-208	157	37	(	(	PUNCT
eurjchem-208	157	38	20	20	NUM
eurjchem-208	157	39	cm3	cm3	NOUN
eurjchem-208	157	40	)	)	PUNCT
eurjchem-208	157	41	in	in	ADP
eurjchem-208	157	42	the	the	DET
eurjchem-208	157	43	presence	presence	NOUN
eurjchem-208	157	44	of	of	ADP
eurjchem-208	157	45	anhydrous	anhydrous	ADJ
eurjchem-208	157	46	zinc	zinc	NOUN
eurjchem-208	157	47	chloride	chloride	NOUN
eurjchem-208	157	48	(	(	PUNCT
eurjchem-208	157	49	1	1	NUM
eurjchem-208	157	50	g	g	NOUN
eurjchem-208	157	51	)	)	PUNCT
eurjchem-208	157	52	,	,	PUNCT
eurjchem-208	157	53	was	be	AUX
eurjchem-208	157	54	refluxed	refluxe	VERB
eurjchem-208	157	55	for	for	ADP
eurjchem-208	157	56	8	8	NUM
eurjchem-208	157	57	h.	h.	NOUN
eurjchem-208	157	58	the	the	DET
eurjchem-208	157	59	mixture	mixture	NOUN
eurjchem-208	157	60	was	be	AUX
eurjchem-208	157	61	cooled	cool	VERB
eurjchem-208	157	62	,	,	PUNCT
eurjchem-208	157	63	and	and	CCONJ
eurjchem-208	157	64	poured	pour	VERB
eurjchem-208	157	65	into	into	ADP
eurjchem-208	157	66	crushed	crush	VERB
eurjchem-208	157	67	ice	ice	NOUN
eurjchem-208	157	68	.	.	PUNCT
eurjchem-208	158	1	the	the	DET
eurjchem-208	158	2	resulting	result	VERB
eurjchem-208	158	3	precipitate	precipitate	NOUN
eurjchem-208	158	4	was	be	AUX
eurjchem-208	158	5	filtered	filter	VERB
eurjchem-208	158	6	off	off	ADP
eurjchem-208	158	7	and	and	CCONJ
eurjchem-208	158	8	crystallized	crystallize	VERB
eurjchem-208	158	9	from	from	ADP
eurjchem-208	158	10	dry	dry	ADJ
eurjchem-208	158	11	benzene	benzene	NOUN
eurjchem-208	158	12	to	to	PART
eurjchem-208	158	13	give	give	VERB
eurjchem-208	158	14	beige	beige	ADJ
eurjchem-208	158	15	crystals	crystal	NOUN
eurjchem-208	158	16	in	in	ADP
eurjchem-208	158	17	45	45	NUM
eurjchem-208	158	18	%	%	NOUN
eurjchem-208	158	19	yield	yield	NOUN
eurjchem-208	158	20	.	.	PUNCT
eurjchem-208	159	1	m.p	m.p	PROPN
eurjchem-208	159	2	.	.	PROPN
eurjchem-208	159	3	:	:	PUNCT
eurjchem-208	160	1	278–280	278–280	NUM
eurjchem-208	160	2	°	°	NOUN
eurjchem-208	160	3	c	c	NOUN
eurjchem-208	160	4	(	(	PUNCT
eurjchem-208	160	5	dec	dec	PROPN
eurjchem-208	160	6	.	.	PROPN
eurjchem-208	160	7	)	)	PUNCT
eurjchem-208	160	8	.	.	PUNCT
eurjchem-208	161	1	method	method	PROPN
eurjchem-208	161	2	b	b	NOUN
eurjchem-208	161	3	:	:	PUNCT
eurjchem-208	161	4	a	a	DET
eurjchem-208	161	5	mixture	mixture	NOUN
eurjchem-208	161	6	of	of	ADP
eurjchem-208	161	7	bis‐(4‐formylpyrazolyl)phosphine	bis‐(4‐formylpyrazolyl)phosphine	NOUN
eurjchem-208	161	8	oxide	oxide	NOUN
eurjchem-208	161	9	4a	4a	X
eurjchem-208	161	10	(	(	PUNCT
eurjchem-208	161	11	0.001	0.001	NUM
eurjchem-208	161	12	mol	mol	NOUN
eurjchem-208	161	13	,	,	PUNCT
eurjchem-208	161	14	0.39	0.39	NUM
eurjchem-208	161	15	g	g	NOUN
eurjchem-208	161	16	)	)	PUNCT
eurjchem-208	161	17	,	,	PUNCT
eurjchem-208	161	18	freshly	freshly	ADV
eurjchem-208	161	19	distillated	distillate	VERB
eurjchem-208	161	20	aniline	aniline	NOUN
eurjchem-208	161	21	(	(	PUNCT
eurjchem-208	161	22	0.002	0.002	NUM
eurjchem-208	161	23	mol	mol	NOUN
eurjchem-208	161	24	,	,	PUNCT
eurjchem-208	161	25	0.186	0.186	NUM
eurjchem-208	161	26	g	g	NOUN
eurjchem-208	161	27	)	)	PUNCT
eurjchem-208	161	28	,	,	PUNCT
eurjchem-208	161	29	thioglycolic	thioglycolic	ADJ
eurjchem-208	161	30	acid	acid	NOUN
eurjchem-208	161	31	(	(	PUNCT
eurjchem-208	161	32	0.0025	0.0025	NUM
eurjchem-208	161	33	mol	mol	NOUN
eurjchem-208	161	34	,	,	PUNCT
eurjchem-208	161	35	0.23	0.23	NUM
eurjchem-208	161	36	g	g	NOUN
eurjchem-208	161	37	)	)	PUNCT
eurjchem-208	161	38	and	and	CCONJ
eurjchem-208	161	39	anhydrous	anhydrous	ADJ
eurjchem-208	161	40	zinc	zinc	NOUN
eurjchem-208	161	41	chloride	chloride	NOUN
eurjchem-208	161	42	(	(	PUNCT
eurjchem-208	161	43	1	1	NUM
eurjchem-208	161	44	g	g	NOUN
eurjchem-208	161	45	)	)	PUNCT
eurjchem-208	161	46	,	,	PUNCT
eurjchem-208	161	47	was	be	AUX
eurjchem-208	161	48	heated	heat	VERB
eurjchem-208	161	49	on	on	ADP
eurjchem-208	161	50	water	water	NOUN
eurjchem-208	161	51	bath	bath	NOUN
eurjchem-208	161	52	for	for	ADP
eurjchem-208	161	53	4	4	NUM
eurjchem-208	161	54	h.	h.	NOUN
eurjchem-208	161	55	the	the	DET
eurjchem-208	161	56	mixture	mixture	NOUN
eurjchem-208	161	57	was	be	AUX
eurjchem-208	161	58	cooled	cool	VERB
eurjchem-208	161	59	,	,	PUNCT
eurjchem-208	161	60	and	and	CCONJ
eurjchem-208	161	61	poured	pour	VERB
eurjchem-208	161	62	into	into	ADP
eurjchem-208	161	63	crushed	crush	VERB
eurjchem-208	161	64	ice	ice	NOUN
eurjchem-208	161	65	.	.	PUNCT
eurjchem-208	162	1	the	the	DET
eurjchem-208	162	2	resulting	result	VERB
eurjchem-208	162	3	precipitate	precipitate	NOUN
eurjchem-208	162	4	was	be	AUX
eurjchem-208	162	5	filtered	filter	VERB
eurjchem-208	162	6	off	off	ADP
eurjchem-208	162	7	and	and	CCONJ
eurjchem-208	162	8	crystallized	crystallize	VERB
eurjchem-208	162	9	from	from	ADP
eurjchem-208	162	10	dry	dry	ADJ
eurjchem-208	162	11	benzene	benzene	NOUN
eurjchem-208	162	12	to	to	PART
eurjchem-208	162	13	give	give	VERB
eurjchem-208	162	14	beige	beige	ADJ
eurjchem-208	162	15	crystals	crystal	NOUN
eurjchem-208	162	16	in	in	ADP
eurjchem-208	162	17	66	66	NUM
eurjchem-208	162	18	%	%	NOUN
eurjchem-208	162	19	yield	yield	NOUN
eurjchem-208	162	20	.	.	PUNCT
eurjchem-208	163	1	m.p	m.p	PROPN
eurjchem-208	163	2	.	.	PROPN
eurjchem-208	163	3	:	:	PUNCT
eurjchem-208	164	1	277–279	277–279	NUM
eurjchem-208	164	2	°	°	ADP
eurjchem-208	164	3	c	c	NOUN
eurjchem-208	164	4	(	(	PUNCT
eurjchem-208	164	5	dec	dec	PROPN
eurjchem-208	164	6	.	.	PROPN
eurjchem-208	164	7	)	)	PUNCT
eurjchem-208	164	8	.	.	PUNCT
eurjchem-208	165	1	ir	ir	PROPN
eurjchem-208	165	2	(	(	PUNCT
eurjchem-208	165	3	kbr	kbr	PROPN
eurjchem-208	165	4	,	,	PUNCT
eurjchem-208	165	5	max	max	PROPN
eurjchem-208	165	6	,	,	PUNCT
eurjchem-208	165	7	cm‐1	cm‐1	NUM
eurjchem-208	165	8	):	):	PUNCT
eurjchem-208	165	9	3059	3059	NUM
eurjchem-208	165	10	(	(	PUNCT
eurjchem-208	165	11	c	c	X
eurjchem-208	165	12	–	–	PUNCT
eurjchem-208	165	13	harom	harom	NOUN
eurjchem-208	165	14	)	)	PUNCT
eurjchem-208	165	15	,	,	PUNCT
eurjchem-208	165	16	2877	2877	NUM
eurjchem-208	165	17	(	(	PUNCT
eurjchem-208	165	18	c	c	NOUN
eurjchem-208	165	19	–	–	PUNCT
eurjchem-208	165	20	haliph	haliph	NOUN
eurjchem-208	165	21	)	)	PUNCT
eurjchem-208	165	22	,	,	PUNCT
eurjchem-208	165	23	2500	2500	NUM
eurjchem-208	165	24	(	(	PUNCT
eurjchem-208	165	25	br	br	NOUN
eurjchem-208	165	26	,	,	PUNCT
eurjchem-208	165	27	p	p	NOUN
eurjchem-208	165	28	–	–	PUNCT
eurjchem-208	165	29	h	h	NOUN
eurjchem-208	165	30	)	)	PUNCT
eurjchem-208	165	31	,	,	PUNCT
eurjchem-208	165	32	1658	1658	NUM
eurjchem-208	165	33	(	(	PUNCT
eurjchem-208	165	34	c	c	NOUN
eurjchem-208	165	35	=	=	NOUN
eurjchem-208	165	36	o	o	NOUN
eurjchem-208	165	37	)	)	PUNCT
eurjchem-208	165	38	,	,	PUNCT
eurjchem-208	165	39	1595	1595	NUM
eurjchem-208	165	40	(	(	PUNCT
eurjchem-208	165	41	c	c	NOUN
eurjchem-208	165	42	=	=	SYM
eurjchem-208	165	43	n	n	NUM
eurjchem-208	165	44	)	)	PUNCT
eurjchem-208	165	45	,	,	PUNCT
eurjchem-208	165	46	1308	1308	NUM
eurjchem-208	165	47	(	(	PUNCT
eurjchem-208	165	48	p	p	NOUN
eurjchem-208	165	49	=	=	NOUN
eurjchem-208	165	50	o	o	NOUN
eurjchem-208	165	51	)	)	PUNCT
eurjchem-208	165	52	.	.	PUNCT
eurjchem-208	166	1	1h	1h	NUM
eurjchem-208	166	2	nmr	nmr	NOUN
eurjchem-208	166	3	(	(	PUNCT
eurjchem-208	166	4	dmso	dmso	NOUN
eurjchem-208	166	5	,	,	PUNCT
eurjchem-208	166	6	δ	δ	PROPN
eurjchem-208	166	7	ppm	ppm	NOUN
eurjchem-208	166	8	):	):	PUNCT
eurjchem-208	166	9	4.46	4.46	NUM
eurjchem-208	166	10	(	(	PUNCT
eurjchem-208	166	11	s	s	PROPN
eurjchem-208	166	12	,	,	PUNCT
eurjchem-208	166	13	4h	4h	NOUN
eurjchem-208	166	14	,	,	PUNCT
eurjchem-208	166	15	ch2	ch2	PROPN
eurjchem-208	166	16	)	)	PUNCT
eurjchem-208	166	17	,	,	PUNCT
eurjchem-208	166	18	5.91	5.91	NUM
eurjchem-208	166	19	(	(	PUNCT
eurjchem-208	166	20	s	s	PROPN
eurjchem-208	166	21	,	,	PUNCT
eurjchem-208	166	22	2h	2h	NUM
eurjchem-208	166	23	,	,	PUNCT
eurjchem-208	166	24	c2	c2	PROPN
eurjchem-208	166	25	–	–	PUNCT
eurjchem-208	166	26	hthiazolidine	hthiazolidine	NOUN
eurjchem-208	166	27	)	)	PUNCT
eurjchem-208	166	28	,	,	PUNCT
eurjchem-208	166	29	7.28(d	7.28(d	PROPN
eurjchem-208	166	30	,	,	PUNCT
eurjchem-208	166	31	1h	1h	NUM
eurjchem-208	166	32	,	,	PUNCT
eurjchem-208	166	33	jph=454	jph=454	PROPN
eurjchem-208	166	34	hz	hz	NOUN
eurjchem-208	166	35	,	,	PUNCT
eurjchem-208	166	36	p	p	NOUN
eurjchem-208	166	37	–	–	PUNCT
eurjchem-208	166	38	h	h	NOUN
eurjchem-208	166	39	)	)	PUNCT
eurjchem-208	166	40	,	,	PUNCT
eurjchem-208	166	41	7.07–8.23	7.07–8.23	NUM
eurjchem-208	166	42	(	(	PUNCT
eurjchem-208	166	43	m	m	PROPN
eurjchem-208	166	44	,	,	PUNCT
eurjchem-208	166	45	20h	20h	NOUN
eurjchem-208	166	46	,	,	PUNCT
eurjchem-208	166	47	ph−h	ph−h	NOUN
eurjchem-208	166	48	)	)	PUNCT
eurjchem-208	166	49	,	,	PUNCT
eurjchem-208	166	50	8.64	8.64	NUM
eurjchem-208	166	51	,	,	PUNCT
eurjchem-208	166	52	8.53	8.53	NUM
eurjchem-208	166	53	(	(	PUNCT
eurjchem-208	166	54	ss	ss	PROPN
eurjchem-208	166	55	,	,	PUNCT
eurjchem-208	166	56	2h	2h	NUM
eurjchem-208	166	57	,	,	PUNCT
eurjchem-208	166	58	c5	c5	PROPN
eurjchem-208	166	59	–	–	PUNCT
eurjchem-208	166	60	hpyrazole	hpyrazole	NOUN
eurjchem-208	166	61	)	)	PUNCT
eurjchem-208	166	62	.	.	PUNCT
eurjchem-208	167	1	anal	anal	PROPN
eurjchem-208	167	2	.	.	PUNCT
eurjchem-208	167	3	calcd	calcd	NOUN
eurjchem-208	167	4	.	.	PUNCT
eurjchem-208	168	1	for	for	ADP
eurjchem-208	168	2	c36h29n6o3ps2	c36h29n6o3ps2	NOUN
eurjchem-208	168	3	(	(	PUNCT
eurjchem-208	168	4	688.77	688.77	NUM
eurjchem-208	168	5	):	):	PUNCT
eurjchem-208	168	6	c	c	X
eurjchem-208	168	7	,	,	PUNCT
eurjchem-208	168	8	62.78	62.78	NUM
eurjchem-208	168	9	;	;	PUNCT
eurjchem-208	168	10	h	h	NOUN
eurjchem-208	168	11	,	,	PUNCT
eurjchem-208	168	12	4.24	4.24	NUM
eurjchem-208	168	13	;	;	PUNCT
eurjchem-208	168	14	n	n	CCONJ
eurjchem-208	168	15	,	,	PUNCT
eurjchem-208	168	16	12.20	12.20	NUM
eurjchem-208	168	17	;	;	PUNCT
eurjchem-208	168	18	s	s	X
eurjchem-208	168	19	,	,	PUNCT
eurjchem-208	168	20	9.31	9.31	NUM
eurjchem-208	168	21	.	.	PUNCT
eurjchem-208	169	1	found	find	VERB
eurjchem-208	169	2	:	:	PUNCT
eurjchem-208	170	1	c	c	X
eurjchem-208	170	2	,	,	PUNCT
eurjchem-208	170	3	62.38	62.38	NUM
eurjchem-208	170	4	;	;	PUNCT
eurjchem-208	170	5	h	h	NOUN
eurjchem-208	170	6	,	,	PUNCT
eurjchem-208	170	7	3.94	3.94	NUM
eurjchem-208	170	8	;	;	PUNCT
eurjchem-208	170	9	n	n	CCONJ
eurjchem-208	170	10	,	,	PUNCT
eurjchem-208	170	11	11.84	11.84	NUM
eurjchem-208	170	12	;	;	PUNCT
eurjchem-208	170	13	s	s	X
eurjchem-208	170	14	,	,	PUNCT
eurjchem-208	170	15	9.03	9.03	NUM
eurjchem-208	170	16	%	%	NOUN
eurjchem-208	170	17	.	.	PUNCT
eurjchem-208	171	1	2.2.8	2.2.8	NUM
eurjchem-208	171	2	.	.	PUNCT
eurjchem-208	172	1	bis{diethyl[phenylamino(3‐phenyl‐1h‐pyrazol‐4‐	bis{diethyl[phenylamino(3‐phenyl‐1h‐pyrazol‐4‐	NOUN
eurjchem-208	172	2	yl)methyl]phosphonate}phosphine	yl)methyl]phosphonate}phosphine	PROPN
eurjchem-208	172	3	oxide	oxide	NOUN
eurjchem-208	172	4	(	(	PUNCT
eurjchem-208	172	5	11	11	NUM
eurjchem-208	172	6	)	)	PUNCT
eurjchem-208	172	7	method	method	NOUN
eurjchem-208	172	8	a	a	PRON
eurjchem-208	172	9	:	:	PUNCT
eurjchem-208	172	10	a	a	DET
eurjchem-208	172	11	mixture	mixture	NOUN
eurjchem-208	172	12	of	of	ADP
eurjchem-208	172	13	bis‐schiff	bis‐schiff	PROPN
eurjchem-208	172	14	's	's	PART
eurjchem-208	172	15	base	base	NOUN
eurjchem-208	172	16	9	9	NUM
eurjchem-208	172	17	(	(	PUNCT
eurjchem-208	172	18	0.001	0.001	NUM
eurjchem-208	172	19	mol	mol	NOUN
eurjchem-208	172	20	,	,	PUNCT
eurjchem-208	172	21	0.54	0.54	NUM
eurjchem-208	172	22	g	g	NOUN
eurjchem-208	172	23	)	)	PUNCT
eurjchem-208	172	24	and	and	CCONJ
eurjchem-208	172	25	diethyl	diethyl	NOUN
eurjchem-208	172	26	phosphite	phosphite	NOUN
eurjchem-208	172	27	(	(	PUNCT
eurjchem-208	172	28	5	5	NUM
eurjchem-208	172	29	cm3	cm3	NOUN
eurjchem-208	172	30	)	)	PUNCT
eurjchem-208	172	31	in	in	ADP
eurjchem-208	172	32	the	the	DET
eurjchem-208	172	33	presence	presence	NOUN
eurjchem-208	172	34	of	of	ADP
eurjchem-208	172	35	boron	boron	NOUN
eurjchem-208	172	36	trifluorideetherate	trifluorideetherate	NOUN
eurjchem-208	172	37	(	(	PUNCT
eurjchem-208	172	38	0.2	0.2	NUM
eurjchem-208	172	39	cm3	cm3	NOUN
eurjchem-208	172	40	)	)	PUNCT
eurjchem-208	172	41	,	,	PUNCT
eurjchem-208	172	42	was	be	AUX
eurjchem-208	172	43	heated	heat	VERB
eurjchem-208	172	44	on	on	ADP
eurjchem-208	172	45	water	water	NOUN
eurjchem-208	172	46	bath	bath	NOUN
eurjchem-208	172	47	for	for	ADP
eurjchem-208	172	48	4	4	NUM
eurjchem-208	172	49	h.	h.	NOUN
eurjchem-208	172	50	the	the	DET
eurjchem-208	172	51	excess	excess	NOUN
eurjchem-208	172	52	of	of	ADP
eurjchem-208	172	53	diethyl	diethyl	NOUN
eurjchem-208	172	54	phosphite	phosphite	NOUN
eurjchem-208	172	55	was	be	AUX
eurjchem-208	172	56	removed	remove	VERB
eurjchem-208	172	57	under	under	ADP
eurjchem-208	172	58	reduced	reduced	ADJ
eurjchem-208	172	59	pressure	pressure	NOUN
eurjchem-208	172	60	.	.	PUNCT
eurjchem-208	173	1	some	some	DET
eurjchem-208	173	2	water	water	NOUN
eurjchem-208	173	3	(	(	PUNCT
eurjchem-208	173	4	5	5	NUM
eurjchem-208	173	5	cm3	cm3	NOUN
eurjchem-208	173	6	)	)	PUNCT
eurjchem-208	173	7	was	be	AUX
eurjchem-208	173	8	added	add	VERB
eurjchem-208	173	9	to	to	ADP
eurjchem-208	173	10	the	the	DET
eurjchem-208	173	11	residue	residue	NOUN
eurjchem-208	173	12	to	to	PART
eurjchem-208	173	13	give	give	VERB
eurjchem-208	173	14	yellow	yellow	ADJ
eurjchem-208	173	15	precipitate	precipitate	NOUN
eurjchem-208	173	16	which	which	PRON
eurjchem-208	173	17	was	be	AUX
eurjchem-208	173	18	filtered	filter	VERB
eurjchem-208	173	19	off	off	ADP
eurjchem-208	173	20	and	and	CCONJ
eurjchem-208	173	21	crystallized	crystallize	VERB
eurjchem-208	173	22	from	from	ADP
eurjchem-208	173	23	dilute	dilute	NOUN
eurjchem-208	173	24	ethanol	ethanol	NOUN
eurjchem-208	173	25	to	to	PART
eurjchem-208	173	26	give	give	VERB
eurjchem-208	173	27	pale	pale	ADJ
eurjchem-208	173	28	yellow	yellow	ADJ
eurjchem-208	173	29	crystals	crystal	NOUN
eurjchem-208	173	30	in	in	ADP
eurjchem-208	173	31	68	68	NUM
eurjchem-208	173	32	%	%	NOUN
eurjchem-208	173	33	yield	yield	NOUN
eurjchem-208	173	34	.	.	PUNCT
eurjchem-208	174	1	m.p	m.p	PROPN
eurjchem-208	174	2	.	.	PROPN
eurjchem-208	174	3	:	:	PUNCT
eurjchem-208	175	1	99–100	99–100	NUM
eurjchem-208	175	2	°	°	PROPN
eurjchem-208	175	3	c	c	PROPN
eurjchem-208	175	4	.	.	PUNCT
eurjchem-208	176	1	28	28	NUM
eurjchem-208	176	2	abdel‐aziz	abdel‐aziz	INTJ
eurjchem-208	176	3	et	et	PROPN
eurjchem-208	176	4	al	al	PROPN
eurjchem-208	176	5	.	.	PUNCT
eurjchem-208	176	6	/	/	SYM
eurjchem-208	176	7	european	european	PROPN
eurjchem-208	176	8	journal	journal	PROPN
eurjchem-208	176	9	of	of	ADP
eurjchem-208	176	10	chemistry	chemistry	NOUN
eurjchem-208	176	11	2	2	NUM
eurjchem-208	176	12	(	(	PUNCT
eurjchem-208	176	13	1	1	NUM
eurjchem-208	176	14	)	)	PUNCT
eurjchem-208	176	15	(	(	PUNCT
eurjchem-208	176	16	2011	2011	NUM
eurjchem-208	176	17	)	)	PUNCT
eurjchem-208	176	18	25‐35	25‐35	NUM
eurjchem-208	176	19	method	method	NOUN
eurjchem-208	176	20	b	b	NOUN
eurjchem-208	176	21	:	:	PUNCT
eurjchem-208	176	22	a	a	DET
eurjchem-208	176	23	mixture	mixture	NOUN
eurjchem-208	176	24	of	of	ADP
eurjchem-208	176	25	bis‐(4‐formylpyrazolyl)phosphine	bis‐(4‐formylpyrazolyl)phosphine	NOUN
eurjchem-208	176	26	oxide	oxide	NOUN
eurjchem-208	176	27	4a	4a	X
eurjchem-208	176	28	(	(	PUNCT
eurjchem-208	176	29	0.001	0.001	NUM
eurjchem-208	176	30	mol	mol	NOUN
eurjchem-208	176	31	,	,	PUNCT
eurjchem-208	176	32	0.39	0.39	NUM
eurjchem-208	176	33	g	g	NOUN
eurjchem-208	176	34	)	)	PUNCT
eurjchem-208	176	35	,	,	PUNCT
eurjchem-208	176	36	freshly	freshly	ADV
eurjchem-208	176	37	distillated	distillate	VERB
eurjchem-208	176	38	aniline	aniline	NOUN
eurjchem-208	176	39	(	(	PUNCT
eurjchem-208	176	40	0.002	0.002	NUM
eurjchem-208	176	41	mol	mol	NOUN
eurjchem-208	176	42	,	,	PUNCT
eurjchem-208	176	43	0.186	0.186	NUM
eurjchem-208	176	44	g	g	NOUN
eurjchem-208	176	45	)	)	PUNCT
eurjchem-208	176	46	,	,	PUNCT
eurjchem-208	176	47	diethyl	diethyl	NOUN
eurjchem-208	176	48	phosphite	phosphite	NOUN
eurjchem-208	176	49	(	(	PUNCT
eurjchem-208	176	50	5	5	NUM
eurjchem-208	176	51	cm3	cm3	NOUN
eurjchem-208	176	52	)	)	PUNCT
eurjchem-208	176	53	,	,	PUNCT
eurjchem-208	176	54	and	and	CCONJ
eurjchem-208	176	55	boron	boron	NOUN
eurjchem-208	176	56	trifluorideetherate	trifluorideetherate	NOUN
eurjchem-208	176	57	(	(	PUNCT
eurjchem-208	176	58	0.2	0.2	NUM
eurjchem-208	176	59	cm3	cm3	NOUN
eurjchem-208	176	60	)	)	PUNCT
eurjchem-208	176	61	,	,	PUNCT
eurjchem-208	176	62	was	be	AUX
eurjchem-208	176	63	heated	heat	VERB
eurjchem-208	176	64	on	on	ADP
eurjchem-208	176	65	water	water	NOUN
eurjchem-208	176	66	bath	bath	NOUN
eurjchem-208	176	67	for	for	ADP
eurjchem-208	176	68	4	4	NUM
eurjchem-208	176	69	h.	h.	NOUN
eurjchem-208	176	70	the	the	DET
eurjchem-208	176	71	excess	excess	NOUN
eurjchem-208	176	72	of	of	ADP
eurjchem-208	176	73	diethyl	diethyl	NOUN
eurjchem-208	176	74	phosphite	phosphite	NOUN
eurjchem-208	176	75	was	be	AUX
eurjchem-208	176	76	removed	remove	VERB
eurjchem-208	176	77	under	under	ADP
eurjchem-208	176	78	reduced	reduced	ADJ
eurjchem-208	176	79	pressure	pressure	NOUN
eurjchem-208	176	80	.	.	PUNCT
eurjchem-208	177	1	some	some	DET
eurjchem-208	177	2	water	water	NOUN
eurjchem-208	177	3	(	(	PUNCT
eurjchem-208	177	4	5	5	NUM
eurjchem-208	177	5	cm3	cm3	NOUN
eurjchem-208	177	6	)	)	PUNCT
eurjchem-208	177	7	was	be	AUX
eurjchem-208	177	8	added	add	VERB
eurjchem-208	177	9	to	to	ADP
eurjchem-208	177	10	the	the	DET
eurjchem-208	177	11	residue	residue	NOUN
eurjchem-208	177	12	to	to	PART
eurjchem-208	177	13	give	give	VERB
eurjchem-208	177	14	yellow	yellow	ADJ
eurjchem-208	177	15	precipitate	precipitate	NOUN
eurjchem-208	177	16	which	which	PRON
eurjchem-208	177	17	was	be	AUX
eurjchem-208	177	18	filtered	filter	VERB
eurjchem-208	177	19	off	off	ADP
eurjchem-208	177	20	and	and	CCONJ
eurjchem-208	177	21	crystallized	crystallize	VERB
eurjchem-208	177	22	from	from	ADP
eurjchem-208	177	23	dilute	dilute	NOUN
eurjchem-208	177	24	ethanol	ethanol	NOUN
eurjchem-208	177	25	to	to	PART
eurjchem-208	177	26	give	give	VERB
eurjchem-208	177	27	pale	pale	ADJ
eurjchem-208	177	28	yellow	yellow	ADJ
eurjchem-208	177	29	crystals	crystal	NOUN
eurjchem-208	177	30	in	in	ADP
eurjchem-208	177	31	72	72	NUM
eurjchem-208	177	32	%	%	NOUN
eurjchem-208	177	33	yield	yield	NOUN
eurjchem-208	177	34	.	.	PUNCT
eurjchem-208	178	1	m.p	m.p	PROPN
eurjchem-208	178	2	.	.	PROPN
eurjchem-208	178	3	:	:	PUNCT
eurjchem-208	179	1	100–101	100–101	NUM
eurjchem-208	179	2	°	°	NUM
eurjchem-208	179	3	c	c	X
eurjchem-208	179	4	.	.	PUNCT
eurjchem-208	180	1	ir	ir	PROPN
eurjchem-208	180	2	(	(	PUNCT
eurjchem-208	180	3	kbr	kbr	PROPN
eurjchem-208	180	4	,	,	PUNCT
eurjchem-208	180	5	max	max	PROPN
eurjchem-208	180	6	,	,	PUNCT
eurjchem-208	180	7	cm‐1	cm‐1	PROPN
eurjchem-208	180	8	):	):	PUNCT
eurjchem-208	180	9	3300	3300	NUM
eurjchem-208	180	10	(	(	PUNCT
eurjchem-208	180	11	nh	nh	NOUN
eurjchem-208	180	12	)	)	PUNCT
eurjchem-208	180	13	,	,	PUNCT
eurjchem-208	180	14	3057	3057	NUM
eurjchem-208	180	15	(	(	PUNCT
eurjchem-208	180	16	c	c	X
eurjchem-208	180	17	–	–	PUNCT
eurjchem-208	180	18	harom	harom	NOUN
eurjchem-208	180	19	)	)	PUNCT
eurjchem-208	180	20	,	,	PUNCT
eurjchem-208	180	21	2983	2983	NUM
eurjchem-208	180	22	,	,	PUNCT
eurjchem-208	180	23	2906	2906	NUM
eurjchem-208	180	24	(	(	PUNCT
eurjchem-208	180	25	c	c	NOUN
eurjchem-208	180	26	–	–	PUNCT
eurjchem-208	180	27	haliph	haliph	NOUN
eurjchem-208	180	28	)	)	PUNCT
eurjchem-208	180	29	,	,	PUNCT
eurjchem-208	180	30	2583	2583	NUM
eurjchem-208	180	31	(	(	PUNCT
eurjchem-208	180	32	p	p	X
eurjchem-208	180	33	–	–	PUNCT
eurjchem-208	180	34	h	h	NOUN
eurjchem-208	180	35	)	)	PUNCT
eurjchem-208	180	36	,	,	PUNCT
eurjchem-208	180	37	1599	1599	NUM
eurjchem-208	180	38	(	(	PUNCT
eurjchem-208	180	39	c	c	NOUN
eurjchem-208	180	40	=	=	SYM
eurjchem-208	180	41	n	n	NUM
eurjchem-208	180	42	)	)	PUNCT
eurjchem-208	180	43	,	,	PUNCT
eurjchem-208	180	44	1536	1536	NUM
eurjchem-208	180	45	(	(	PUNCT
eurjchem-208	180	46	c	c	NOUN
eurjchem-208	180	47	=	=	SYM
eurjchem-208	180	48	c	c	NOUN
eurjchem-208	180	49	)	)	PUNCT
eurjchem-208	180	50	,	,	PUNCT
eurjchem-208	180	51	1287	1287	NUM
eurjchem-208	180	52	,	,	PUNCT
eurjchem-208	180	53	1233	1233	NUM
eurjchem-208	180	54	(	(	PUNCT
eurjchem-208	180	55	2	2	NUM
eurjchem-208	180	56	p	p	NOUN
eurjchem-208	180	57	=	=	NOUN
eurjchem-208	180	58	o	o	NOUN
eurjchem-208	180	59	)	)	PUNCT
eurjchem-208	180	60	,	,	PUNCT
eurjchem-208	180	61	1049	1049	NUM
eurjchem-208	180	62	(	(	PUNCT
eurjchem-208	180	63	p	p	X
eurjchem-208	180	64	–	–	PUNCT
eurjchem-208	180	65	o	o	NOUN
eurjchem-208	180	66	–	–	PUNCT
eurjchem-208	180	67	c	c	NOUN
eurjchem-208	180	68	)	)	PUNCT
eurjchem-208	180	69	.	.	PUNCT
eurjchem-208	181	1	1h	1h	NUM
eurjchem-208	181	2	nmr	nmr	NOUN
eurjchem-208	181	3	(	(	PUNCT
eurjchem-208	181	4	dmso	dmso	NOUN
eurjchem-208	181	5	,	,	PUNCT
eurjchem-208	181	6	δ	δ	PROPN
eurjchem-208	181	7	ppm	ppm	VERB
eurjchem-208	181	8	):	):	PUNCT
eurjchem-208	181	9	1.07	1.07	NUM
eurjchem-208	181	10	(	(	PUNCT
eurjchem-208	181	11	t	t	PROPN
eurjchem-208	181	12	,	,	PUNCT
eurjchem-208	181	13	12h	12h	NUM
eurjchem-208	181	14	,	,	PUNCT
eurjchem-208	181	15	j=6.8	j=6.8	NOUN
eurjchem-208	181	16	hz	hz	VERB
eurjchem-208	181	17	,	,	PUNCT
eurjchem-208	181	18	ch3ch2o	ch3ch2o	NOUN
eurjchem-208	181	19	)	)	PUNCT
eurjchem-208	181	20	,	,	PUNCT
eurjchem-208	181	21	3.96	3.96	NUM
eurjchem-208	181	22	(	(	PUNCT
eurjchem-208	181	23	q	q	NOUN
eurjchem-208	181	24	,	,	PUNCT
eurjchem-208	181	25	8h	8h	PROPN
eurjchem-208	181	26	,	,	PUNCT
eurjchem-208	181	27	j=6.8	j=6.8	NOUN
eurjchem-208	181	28	hz	hz	VERB
eurjchem-208	181	29	,	,	PUNCT
eurjchem-208	181	30	ch3ch2o	ch3ch2o	NOUN
eurjchem-208	181	31	)	)	PUNCT
eurjchem-208	181	32	,	,	PUNCT
eurjchem-208	181	33	4.91	4.91	NUM
eurjchem-208	181	34	(	(	PUNCT
eurjchem-208	181	35	d	d	PROPN
eurjchem-208	181	36	,	,	PUNCT
eurjchem-208	181	37	2h	2h	NUM
eurjchem-208	181	38	,	,	PUNCT
eurjchem-208	181	39	jpch=18.4	jpch=18.4	NOUN
eurjchem-208	181	40	hz	hz	NOUN
eurjchem-208	181	41	,	,	PUNCT
eurjchem-208	181	42	ch	ch	NOUN
eurjchem-208	181	43	–	–	PUNCT
eurjchem-208	181	44	p	p	NOUN
eurjchem-208	181	45	)	)	PUNCT
eurjchem-208	181	46	,	,	PUNCT
eurjchem-208	181	47	6.60–7.97	6.60–7.97	NUM
eurjchem-208	181	48	(	(	PUNCT
eurjchem-208	181	49	m	m	PROPN
eurjchem-208	181	50	,	,	PUNCT
eurjchem-208	181	51	20h	20h	NOUN
eurjchem-208	181	52	,	,	PUNCT
eurjchem-208	181	53	ph−h	ph−h	NOUN
eurjchem-208	181	54	)	)	PUNCT
eurjchem-208	181	55	,	,	PUNCT
eurjchem-208	181	56	7.40	7.40	NUM
eurjchem-208	181	57	(	(	PUNCT
eurjchem-208	181	58	d	d	PROPN
eurjchem-208	181	59	,	,	PUNCT
eurjchem-208	181	60	1h	1h	NUM
eurjchem-208	181	61	,	,	PUNCT
eurjchem-208	181	62	jph=498	jph=498	PROPN
eurjchem-208	181	63	hz	hz	VERB
eurjchem-208	181	64	,	,	PUNCT
eurjchem-208	181	65	p	p	NOUN
eurjchem-208	181	66	–	–	PUNCT
eurjchem-208	181	67	h	h	NOUN
eurjchem-208	181	68	)	)	PUNCT
eurjchem-208	181	69	,	,	PUNCT
eurjchem-208	181	70	8.25	8.25	NUM
eurjchem-208	181	71	(	(	PUNCT
eurjchem-208	181	72	s	s	PROPN
eurjchem-208	181	73	,	,	PUNCT
eurjchem-208	181	74	2h	2h	NUM
eurjchem-208	181	75	,	,	PUNCT
eurjchem-208	181	76	nh	nh	PROPN
eurjchem-208	181	77	exchangeable	exchangeable	ADJ
eurjchem-208	181	78	with	with	ADP
eurjchem-208	181	79	d2o	d2o	NOUN
eurjchem-208	181	80	)	)	PUNCT
eurjchem-208	181	81	,	,	PUNCT
eurjchem-208	181	82	8.65	8.65	NUM
eurjchem-208	181	83	(	(	PUNCT
eurjchem-208	181	84	s	s	PROPN
eurjchem-208	181	85	,	,	PUNCT
eurjchem-208	181	86	2h	2h	NUM
eurjchem-208	181	87	,	,	PUNCT
eurjchem-208	181	88	c5	c5	PROPN
eurjchem-208	181	89	–	–	PUNCT
eurjchem-208	181	90	hpyrazole	hpyrazole	NOUN
eurjchem-208	181	91	)	)	PUNCT
eurjchem-208	181	92	.	.	PUNCT
eurjchem-208	182	1	13c	13c	NOUN
eurjchem-208	182	2	nmr	nmr	NOUN
eurjchem-208	182	3	(	(	PUNCT
eurjchem-208	182	4	dmso	dmso	NOUN
eurjchem-208	182	5	,	,	PUNCT
eurjchem-208	182	6	δ	δ	PROPN
eurjchem-208	182	7	ppm	ppm	VERB
eurjchem-208	182	8	):	):	PUNCT
eurjchem-208	182	9	16.0	16.0	NUM
eurjchem-208	182	10	(	(	PUNCT
eurjchem-208	182	11	j=6.9	j=6.9	PROPN
eurjchem-208	182	12	hz	hz	PROPN
eurjchem-208	182	13	,	,	PUNCT
eurjchem-208	182	14	ch3ch2o	ch3ch2o	NOUN
eurjchem-208	182	15	)	)	PUNCT
eurjchem-208	182	16	,	,	PUNCT
eurjchem-208	182	17	46.1	46.1	NUM
eurjchem-208	182	18	(	(	PUNCT
eurjchem-208	182	19	d	d	PROPN
eurjchem-208	182	20	,	,	PUNCT
eurjchem-208	182	21	jpc=161	jpc=161	PROPN
eurjchem-208	182	22	hz	hz	PROPN
eurjchem-208	182	23	,	,	PUNCT
eurjchem-208	182	24	ch	ch	NOUN
eurjchem-208	182	25	–	–	PUNCT
eurjchem-208	182	26	p	p	NOUN
eurjchem-208	182	27	)	)	PUNCT
eurjchem-208	182	28	,	,	PUNCT
eurjchem-208	182	29	62.7	62.7	NUM
eurjchem-208	182	30	(	(	PUNCT
eurjchem-208	182	31	j=6.9	j=6.9	PROPN
eurjchem-208	182	32	hz	hz	PROPN
eurjchem-208	182	33	,	,	PUNCT
eurjchem-208	182	34	ch3ch2o	ch3ch2o	NOUN
eurjchem-208	182	35	)	)	PUNCT
eurjchem-208	182	36	,	,	PUNCT
eurjchem-208	182	37	118.0	118.0	NUM
eurjchem-208	182	38	(	(	PUNCT
eurjchem-208	182	39	c4	c4	NOUN
eurjchem-208	182	40	pyrazole	pyrazole	NOUN
eurjchem-208	182	41	)	)	PUNCT
eurjchem-208	182	42	,	,	PUNCT
eurjchem-208	182	43	126.5–139.0	126.5–139.0	NUM
eurjchem-208	182	44	(	(	PUNCT
eurjchem-208	182	45	phenyl	phenyl	NOUN
eurjchem-208	182	46	carbons	carbon	NOUN
eurjchem-208	182	47	)	)	PUNCT
eurjchem-208	182	48	,	,	PUNCT
eurjchem-208	182	49	146.7	146.7	NUM
eurjchem-208	182	50	(	(	PUNCT
eurjchem-208	182	51	c5pyrazole	c5pyrazole	NOUN
eurjchem-208	182	52	)	)	PUNCT
eurjchem-208	182	53	,	,	PUNCT
eurjchem-208	182	54	151.2	151.2	NUM
eurjchem-208	182	55	(	(	PUNCT
eurjchem-208	182	56	c3pyrazole	c3pyrazole	PROPN
eurjchem-208	182	57	)	)	PUNCT
eurjchem-208	182	58	.	.	PUNCT
eurjchem-208	183	1	31p	31p	NOUN
eurjchem-208	183	2	nmr(dmso	nmr(dmso	NUM
eurjchem-208	183	3	,	,	PUNCT
eurjchem-208	183	4	δ	δ	PROPN
eurjchem-208	183	5	ppm	ppm	VERB
eurjchem-208	183	6	):	):	PUNCT
eurjchem-208	183	7	8.2	8.2	NUM
eurjchem-208	183	8	(	(	PUNCT
eurjchem-208	183	9	o	o	NOUN
eurjchem-208	183	10	=	=	SYM
eurjchem-208	183	11	p	p	NOUN
eurjchem-208	183	12	–	–	PUNCT
eurjchem-208	183	13	h	h	NOUN
eurjchem-208	183	14	)	)	PUNCT
eurjchem-208	183	15	,	,	PUNCT
eurjchem-208	183	16	21.5	21.5	NUM
eurjchem-208	183	17	(	(	PUNCT
eurjchem-208	183	18	eto	eto	PROPN
eurjchem-208	183	19	–	–	PUNCT
eurjchem-208	183	20	p	p	X
eurjchem-208	183	21	=	=	NOUN
eurjchem-208	183	22	o	o	NOUN
eurjchem-208	183	23	)	)	PUNCT
eurjchem-208	183	24	.	.	PUNCT
eurjchem-208	184	1	anal	anal	PROPN
eurjchem-208	184	2	.	.	PUNCT
eurjchem-208	184	3	calcd	calcd	NOUN
eurjchem-208	184	4	.	.	PUNCT
eurjchem-208	185	1	for	for	ADP
eurjchem-208	185	2	c40h47n6o7p3	c40h47n6o7p3	NOUN
eurjchem-208	185	3	(	(	PUNCT
eurjchem-208	185	4	816.78	816.78	NUM
eurjchem-208	185	5	):	):	PUNCT
eurjchem-208	185	6	c	c	X
eurjchem-208	185	7	,	,	PUNCT
eurjchem-208	185	8	58.82	58.82	NUM
eurjchem-208	185	9	;	;	PUNCT
eurjchem-208	185	10	h	h	NOUN
eurjchem-208	185	11	,	,	PUNCT
eurjchem-208	185	12	5.80	5.80	NUM
eurjchem-208	185	13	;	;	PUNCT
eurjchem-208	185	14	n	n	CCONJ
eurjchem-208	185	15	,	,	PUNCT
eurjchem-208	185	16	10.29	10.29	NUM
eurjchem-208	185	17	.	.	PUNCT
eurjchem-208	185	18	found	find	VERB
eurjchem-208	185	19	:	:	PUNCT
eurjchem-208	186	1	c	c	X
eurjchem-208	186	2	,	,	PUNCT
eurjchem-208	186	3	58.61	58.61	NUM
eurjchem-208	186	4	;	;	PUNCT
eurjchem-208	186	5	h	h	NOUN
eurjchem-208	186	6	,	,	PUNCT
eurjchem-208	186	7	5.42	5.42	NUM
eurjchem-208	186	8	;	;	PUNCT
eurjchem-208	186	9	n	n	CCONJ
eurjchem-208	186	10	,	,	PUNCT
eurjchem-208	186	11	9.79	9.79	NUM
eurjchem-208	186	12	%	%	NOUN
eurjchem-208	186	13	.	.	PUNCT
eurjchem-208	187	1	2.2.9	2.2.9	X
eurjchem-208	187	2	.	.	PUNCT
eurjchem-208	188	1	bis{3‐phenyl‐4‐(1‐oxo‐1‐phenylprop‐2‐en‐3‐yl)‐1h‐	bis{3‐phenyl‐4‐(1‐oxo‐1‐phenylprop‐2‐en‐3‐yl)‐1h‐	VERB
eurjchem-208	188	2	pyrazol‐1‐yl}phosphine	pyrazol‐1‐yl}phosphine	ADJ
eurjchem-208	188	3	oxide	oxide	NOUN
eurjchem-208	188	4	(	(	PUNCT
eurjchem-208	188	5	12	12	NUM
eurjchem-208	188	6	)	)	PUNCT
eurjchem-208	188	7	a	a	DET
eurjchem-208	188	8	mixture	mixture	NOUN
eurjchem-208	188	9	of	of	ADP
eurjchem-208	188	10	bis‐(4‐formylpyrazolyl)phosphine	bis‐(4‐formylpyrazolyl)phosphine	NOUN
eurjchem-208	188	11	oxide	oxide	NOUN
eurjchem-208	188	12	4a	4a	X
eurjchem-208	188	13	(	(	PUNCT
eurjchem-208	188	14	0.001	0.001	NUM
eurjchem-208	188	15	mol	mol	NOUN
eurjchem-208	188	16	,	,	PUNCT
eurjchem-208	188	17	0.39	0.39	NUM
eurjchem-208	188	18	g	g	NOUN
eurjchem-208	188	19	)	)	PUNCT
eurjchem-208	188	20	and	and	CCONJ
eurjchem-208	188	21	phenacyltriphenylphosphonium	phenacyltriphenylphosphonium	NOUN
eurjchem-208	188	22	bromide	bromide	NOUN
eurjchem-208	188	23	(	(	PUNCT
eurjchem-208	188	24	0.002	0.002	NUM
eurjchem-208	188	25	mol	mol	NOUN
eurjchem-208	188	26	,	,	PUNCT
eurjchem-208	188	27	0.92	0.92	NUM
eurjchem-208	188	28	g	g	NOUN
eurjchem-208	188	29	)	)	PUNCT
eurjchem-208	188	30	in	in	ADP
eurjchem-208	188	31	dry	dry	ADJ
eurjchem-208	188	32	dioxane	dioxane	NOUN
eurjchem-208	188	33	(	(	PUNCT
eurjchem-208	188	34	20	20	NUM
eurjchem-208	188	35	cm3	cm3	NOUN
eurjchem-208	188	36	)	)	PUNCT
eurjchem-208	188	37	in	in	ADP
eurjchem-208	188	38	the	the	DET
eurjchem-208	188	39	presence	presence	NOUN
eurjchem-208	188	40	of	of	ADP
eurjchem-208	188	41	few	few	ADJ
eurjchem-208	188	42	drops	drop	NOUN
eurjchem-208	188	43	of	of	ADP
eurjchem-208	188	44	triethylamine	triethylamine	NOUN
eurjchem-208	188	45	was	be	AUX
eurjchem-208	188	46	refluxed	refluxe	VERB
eurjchem-208	188	47	for	for	ADP
eurjchem-208	188	48	6	6	NUM
eurjchem-208	188	49	h.	h.	NOUN
eurjchem-208	188	50	the	the	DET
eurjchem-208	188	51	reaction	reaction	NOUN
eurjchem-208	188	52	mixture	mixture	NOUN
eurjchem-208	188	53	was	be	AUX
eurjchem-208	188	54	cooled	cool	VERB
eurjchem-208	188	55	;	;	PUNCT
eurjchem-208	188	56	the	the	DET
eurjchem-208	188	57	resulting	result	VERB
eurjchem-208	188	58	precipitate	precipitate	NOUN
eurjchem-208	188	59	was	be	AUX
eurjchem-208	188	60	filtered	filter	VERB
eurjchem-208	188	61	off	off	ADP
eurjchem-208	188	62	and	and	CCONJ
eurjchem-208	188	63	crystallized	crystallize	VERB
eurjchem-208	188	64	from	from	ADP
eurjchem-208	188	65	dilute	dilute	ADJ
eurjchem-208	188	66	dimethylformamide	dimethylformamide	NOUN
eurjchem-208	188	67	to	to	PART
eurjchem-208	188	68	give	give	VERB
eurjchem-208	188	69	pale	pale	ADJ
eurjchem-208	188	70	yellow	yellow	ADJ
eurjchem-208	188	71	crystals	crystal	NOUN
eurjchem-208	188	72	in	in	ADP
eurjchem-208	188	73	71	71	NUM
eurjchem-208	188	74	%	%	NOUN
eurjchem-208	188	75	yield	yield	NOUN
eurjchem-208	188	76	.	.	PUNCT
eurjchem-208	189	1	m.p	m.p	PROPN
eurjchem-208	189	2	.	.	PROPN
eurjchem-208	189	3	:	:	PUNCT
eurjchem-208	190	1	128−130	128−130	NUM
eurjchem-208	190	2	oc	oc	X
eurjchem-208	190	3	.	.	PROPN
eurjchem-208	190	4	ir	ir	PROPN
eurjchem-208	190	5	(	(	PUNCT
eurjchem-208	190	6	kbr	kbr	PROPN
eurjchem-208	190	7	,	,	PUNCT
eurjchem-208	190	8	max	max	PROPN
eurjchem-208	190	9	,	,	PUNCT
eurjchem-208	190	10	cm‐1	cm‐1	PROPN
eurjchem-208	190	11	):	):	PUNCT
eurjchem-208	190	12	3052	3052	NUM
eurjchem-208	190	13	(	(	PUNCT
eurjchem-208	190	14	c	c	X
eurjchem-208	190	15	–	–	PUNCT
eurjchem-208	190	16	harom	harom	NOUN
eurjchem-208	190	17	)	)	PUNCT
eurjchem-208	190	18	,	,	PUNCT
eurjchem-208	190	19	2500	2500	NUM
eurjchem-208	190	20	(	(	PUNCT
eurjchem-208	190	21	br	br	NOUN
eurjchem-208	190	22	,	,	PUNCT
eurjchem-208	190	23	p	p	NOUN
eurjchem-208	190	24	–	–	PUNCT
eurjchem-208	190	25	h	h	NOUN
eurjchem-208	190	26	)	)	PUNCT
eurjchem-208	190	27	,	,	PUNCT
eurjchem-208	190	28	1687	1687	NUM
eurjchem-208	190	29	(	(	PUNCT
eurjchem-208	190	30	c	c	NOUN
eurjchem-208	190	31	=	=	NOUN
eurjchem-208	190	32	o	o	NOUN
eurjchem-208	190	33	)	)	PUNCT
eurjchem-208	190	34	,	,	PUNCT
eurjchem-208	190	35	1599	1599	NUM
eurjchem-208	190	36	(	(	PUNCT
eurjchem-208	190	37	ch	ch	NOUN
eurjchem-208	190	38	=	=	NOUN
eurjchem-208	190	39	ch	ch	NOUN
eurjchem-208	190	40	)	)	PUNCT
eurjchem-208	190	41	,	,	PUNCT
eurjchem-208	190	42	1562	1562	NUM
eurjchem-208	190	43	(	(	PUNCT
eurjchem-208	190	44	c	c	NOUN
eurjchem-208	190	45	=	=	SYM
eurjchem-208	190	46	n	n	NUM
eurjchem-208	190	47	)	)	PUNCT
eurjchem-208	190	48	,	,	PUNCT
eurjchem-208	190	49	1529	1529	NUM
eurjchem-208	190	50	(	(	PUNCT
eurjchem-208	190	51	c	c	X
eurjchem-208	190	52	=	=	SYM
eurjchem-208	190	53	c	c	NOUN
eurjchem-208	190	54	)	)	PUNCT
eurjchem-208	190	55	,	,	PUNCT
eurjchem-208	190	56	1215	1215	NUM
eurjchem-208	190	57	(	(	PUNCT
eurjchem-208	190	58	p	p	NOUN
eurjchem-208	190	59	=	=	NOUN
eurjchem-208	190	60	o	o	NOUN
eurjchem-208	190	61	)	)	PUNCT
eurjchem-208	190	62	.	.	PUNCT
eurjchem-208	191	1	1h	1h	NUM
eurjchem-208	191	2	nmr	nmr	NOUN
eurjchem-208	191	3	(	(	PUNCT
eurjchem-208	191	4	dmso	dmso	NOUN
eurjchem-208	191	5	,	,	PUNCT
eurjchem-208	191	6	δ	δ	PROPN
eurjchem-208	191	7	ppm	ppm	NOUN
eurjchem-208	191	8	):	):	PUNCT
eurjchem-208	191	9	7.41–7.73	7.41–7.73	NUM
eurjchem-208	191	10	(	(	PUNCT
eurjchem-208	191	11	m	m	PROPN
eurjchem-208	191	12	,	,	PUNCT
eurjchem-208	191	13	16h	16h	NUM
eurjchem-208	191	14	,	,	PUNCT
eurjchem-208	191	15	ph−h	ph−h	NOUN
eurjchem-208	191	16	)	)	PUNCT
eurjchem-208	191	17	,	,	PUNCT
eurjchem-208	191	18	7.78	7.78	NUM
eurjchem-208	191	19	(	(	PUNCT
eurjchem-208	191	20	d	d	PROPN
eurjchem-208	191	21	,	,	PUNCT
eurjchem-208	191	22	2h	2h	NUM
eurjchem-208	191	23	,	,	PUNCT
eurjchem-208	191	24	j=13.8	j=13.8	PROPN
eurjchem-208	191	25	hz	hz	PROPN
eurjchem-208	191	26	,	,	PUNCT
eurjchem-208	191	27	ch	ch	NOUN
eurjchem-208	191	28	=	=	NOUN
eurjchem-208	191	29	ch	ch	NOUN
eurjchem-208	191	30	–	–	PUNCT
eurjchem-208	191	31	c	c	NOUN
eurjchem-208	191	32	=	=	NOUN
eurjchem-208	191	33	o	o	NOUN
eurjchem-208	191	34	)	)	PUNCT
eurjchem-208	191	35	,	,	PUNCT
eurjchem-208	191	36	7.83–7.96	7.83–7.96	NUM
eurjchem-208	191	37	(	(	PUNCT
eurjchem-208	191	38	m	m	PROPN
eurjchem-208	191	39	,	,	PUNCT
eurjchem-208	191	40	4h	4h	NOUN
eurjchem-208	191	41	,	,	PUNCT
eurjchem-208	191	42	ph−h	ph−h	NOUN
eurjchem-208	191	43	)	)	PUNCT
eurjchem-208	191	44	,	,	PUNCT
eurjchem-208	191	45	8.09	8.09	NUM
eurjchem-208	191	46	(	(	PUNCT
eurjchem-208	191	47	d	d	PROPN
eurjchem-208	191	48	,	,	PUNCT
eurjchem-208	191	49	2h	2h	NUM
eurjchem-208	191	50	,	,	PUNCT
eurjchem-208	191	51	j=13.8	j=13.8	PROPN
eurjchem-208	191	52	hz	hz	PROPN
eurjchem-208	191	53	,	,	PUNCT
eurjchem-208	191	54	ch	ch	NOUN
eurjchem-208	191	55	=	=	NOUN
eurjchem-208	191	56	ch	ch	NOUN
eurjchem-208	191	57	–	–	PUNCT
eurjchem-208	191	58	c	c	NOUN
eurjchem-208	191	59	=	=	NOUN
eurjchem-208	191	60	o	o	NOUN
eurjchem-208	191	61	)	)	PUNCT
eurjchem-208	191	62	,	,	PUNCT
eurjchem-208	191	63	8.36	8.36	NUM
eurjchem-208	191	64	(	(	PUNCT
eurjchem-208	191	65	d	d	PROPN
eurjchem-208	191	66	,	,	PUNCT
eurjchem-208	191	67	1h	1h	NUM
eurjchem-208	191	68	,	,	PUNCT
eurjchem-208	191	69	jph=638	jph=638	PROPN
eurjchem-208	191	70	hz	hz	PROPN
eurjchem-208	191	71	,	,	PUNCT
eurjchem-208	191	72	p	p	NOUN
eurjchem-208	191	73	–	–	PUNCT
eurjchem-208	191	74	h	h	NOUN
eurjchem-208	191	75	)	)	PUNCT
eurjchem-208	191	76	,	,	PUNCT
eurjchem-208	191	77	8.62	8.62	NUM
eurjchem-208	191	78	(	(	PUNCT
eurjchem-208	191	79	s	s	PROPN
eurjchem-208	191	80	,	,	PUNCT
eurjchem-208	191	81	2h	2h	NUM
eurjchem-208	191	82	,	,	PUNCT
eurjchem-208	191	83	c5	c5	PROPN
eurjchem-208	191	84	–	–	PUNCT
eurjchem-208	191	85	hpyrazole	hpyrazole	NOUN
eurjchem-208	191	86	)	)	PUNCT
eurjchem-208	191	87	.	.	PUNCT
eurjchem-208	192	1	13c	13c	NOUN
eurjchem-208	192	2	nmr	nmr	NOUN
eurjchem-208	192	3	(	(	PUNCT
eurjchem-208	192	4	dmso	dmso	NOUN
eurjchem-208	192	5	,	,	PUNCT
eurjchem-208	192	6	δ	δ	PROPN
eurjchem-208	192	7	ppm	ppm	VERB
eurjchem-208	192	8	):	):	PUNCT
eurjchem-208	192	9	118.7	118.7	NUM
eurjchem-208	192	10	(	(	PUNCT
eurjchem-208	192	11	ch	ch	NOUN
eurjchem-208	192	12	=	=	NOUN
eurjchem-208	192	13	ch	ch	NOUN
eurjchem-208	192	14	–	–	PUNCT
eurjchem-208	192	15	c	c	NOUN
eurjchem-208	192	16	=	=	NOUN
eurjchem-208	192	17	o	o	NOUN
eurjchem-208	192	18	)	)	PUNCT
eurjchem-208	192	19	,	,	PUNCT
eurjchem-208	192	20	121.6	121.6	NUM
eurjchem-208	192	21	(	(	PUNCT
eurjchem-208	192	22	c4pyrazole	c4pyrazole	PROPN
eurjchem-208	192	23	)	)	PUNCT
eurjchem-208	192	24	,	,	PUNCT
eurjchem-208	192	25	127.9–137.0	127.9–137.0	NUM
eurjchem-208	192	26	(	(	PUNCT
eurjchem-208	192	27	phenyl	phenyl	NOUN
eurjchem-208	192	28	carbons	carbon	NOUN
eurjchem-208	192	29	)	)	PUNCT
eurjchem-208	192	30	,	,	PUNCT
eurjchem-208	192	31	138.0	138.0	NUM
eurjchem-208	192	32	(	(	PUNCT
eurjchem-208	192	33	ch	ch	NOUN
eurjchem-208	192	34	=	=	NOUN
eurjchem-208	192	35	ch	ch	NOUN
eurjchem-208	192	36	–	–	PUNCT
eurjchem-208	192	37	c	c	NOUN
eurjchem-208	192	38	=	=	NOUN
eurjchem-208	192	39	o	o	NOUN
eurjchem-208	192	40	)	)	PUNCT
eurjchem-208	192	41	,	,	PUNCT
eurjchem-208	192	42	139.0	139.0	NUM
eurjchem-208	192	43	(	(	PUNCT
eurjchem-208	192	44	c5pyrazole	c5pyrazole	NOUN
eurjchem-208	192	45	)	)	PUNCT
eurjchem-208	192	46	,	,	PUNCT
eurjchem-208	192	47	153.0	153.0	NUM
eurjchem-208	192	48	(	(	PUNCT
eurjchem-208	192	49	c3pyrazole	c3pyrazole	PROPN
eurjchem-208	192	50	)	)	PUNCT
eurjchem-208	192	51	,	,	PUNCT
eurjchem-208	192	52	188.0	188.0	NUM
eurjchem-208	192	53	(	(	PUNCT
eurjchem-208	192	54	c	c	NOUN
eurjchem-208	192	55	=	=	NOUN
eurjchem-208	192	56	o	o	NOUN
eurjchem-208	192	57	)	)	PUNCT
eurjchem-208	192	58	.	.	PUNCT
eurjchem-208	193	1	ms	ms	NOUN
eurjchem-208	193	2	(	(	PUNCT
eurjchem-208	193	3	m	m	PROPN
eurjchem-208	193	4	/	/	SYM
eurjchem-208	193	5	e	e	NOUN
eurjchem-208	193	6	,	,	PUNCT
eurjchem-208	193	7	%	%	INTJ
eurjchem-208	193	8	):	):	PUNCT
eurjchem-208	193	9	414	414	NUM
eurjchem-208	193	10	(	(	PUNCT
eurjchem-208	193	11	m+–2ph	m+–2ph	NOUN
eurjchem-208	193	12	,	,	PUNCT
eurjchem-208	193	13	–	–	PUNCT
eurjchem-208	193	14	co	co	NOUN
eurjchem-208	193	15	,	,	PUNCT
eurjchem-208	193	16	0.1	0.1	NUM
eurjchem-208	193	17	%	%	NOUN
eurjchem-208	193	18	)	)	PUNCT
eurjchem-208	193	19	,	,	PUNCT
eurjchem-208	193	20	363	363	NUM
eurjchem-208	193	21	(	(	PUNCT
eurjchem-208	193	22	0.3	0.3	NUM
eurjchem-208	193	23	)	)	PUNCT
eurjchem-208	193	24	,	,	PUNCT
eurjchem-208	193	25	293	293	NUM
eurjchem-208	193	26	(	(	PUNCT
eurjchem-208	193	27	14	14	NUM
eurjchem-208	193	28	)	)	PUNCT
eurjchem-208	193	29	,	,	PUNCT
eurjchem-208	193	30	231	231	NUM
eurjchem-208	193	31	(	(	PUNCT
eurjchem-208	193	32	3	3	NUM
eurjchem-208	193	33	)	)	PUNCT
eurjchem-208	193	34	,	,	PUNCT
eurjchem-208	193	35	168	168	NUM
eurjchem-208	193	36	(	(	PUNCT
eurjchem-208	193	37	14	14	NUM
eurjchem-208	193	38	)	)	PUNCT
eurjchem-208	193	39	,	,	PUNCT
eurjchem-208	193	40	149	149	NUM
eurjchem-208	193	41	(	(	PUNCT
eurjchem-208	193	42	86	86	NUM
eurjchem-208	193	43	)	)	PUNCT
eurjchem-208	193	44	,	,	PUNCT
eurjchem-208	193	45	94	94	NUM
eurjchem-208	193	46	(	(	PUNCT
eurjchem-208	193	47	35	35	NUM
eurjchem-208	193	48	)	)	PUNCT
eurjchem-208	193	49	,	,	PUNCT
eurjchem-208	193	50	85	85	NUM
eurjchem-208	193	51	(	(	PUNCT
eurjchem-208	193	52	71	71	NUM
eurjchem-208	193	53	)	)	PUNCT
eurjchem-208	193	54	,	,	PUNCT
eurjchem-208	193	55	77	77	NUM
eurjchem-208	193	56	(	(	PUNCT
eurjchem-208	193	57	2	2	NUM
eurjchem-208	193	58	)	)	PUNCT
eurjchem-208	193	59	,	,	PUNCT
eurjchem-208	193	60	71	71	NUM
eurjchem-208	193	61	(	(	PUNCT
eurjchem-208	193	62	55	55	NUM
eurjchem-208	193	63	)	)	PUNCT
eurjchem-208	193	64	,	,	PUNCT
eurjchem-208	193	65	57	57	NUM
eurjchem-208	193	66	(	(	PUNCT
eurjchem-208	193	67	100	100	NUM
eurjchem-208	193	68	)	)	PUNCT
eurjchem-208	193	69	.	.	PUNCT
eurjchem-208	194	1	anal	anal	PROPN
eurjchem-208	194	2	.	.	PUNCT
eurjchem-208	194	3	calcd	calcd	NOUN
eurjchem-208	194	4	.	.	PUNCT
eurjchem-208	195	1	for	for	ADP
eurjchem-208	195	2	c36h27n4o3p	c36h27n4o3p	NUM
eurjchem-208	195	3	(	(	PUNCT
eurjchem-208	195	4	594.59	594.59	NUM
eurjchem-208	195	5	):	):	PUNCT
eurjchem-208	195	6	c	c	NOUN
eurjchem-208	195	7	,	,	PUNCT
eurjchem-208	195	8	72.72	72.72	NUM
eurjchem-208	195	9	;	;	PUNCT
eurjchem-208	195	10	h	h	NOUN
eurjchem-208	195	11	,	,	PUNCT
eurjchem-208	195	12	4.58	4.58	NUM
eurjchem-208	195	13	;	;	PUNCT
eurjchem-208	195	14	n	n	CCONJ
eurjchem-208	195	15	,	,	PUNCT
eurjchem-208	195	16	9.42	9.42	NUM
eurjchem-208	195	17	.	.	PUNCT
eurjchem-208	195	18	found	find	VERB
eurjchem-208	195	19	:	:	PUNCT
eurjchem-208	196	1	c	c	X
eurjchem-208	196	2	,	,	PUNCT
eurjchem-208	196	3	72.35	72.35	NUM
eurjchem-208	196	4	;	;	PUNCT
eurjchem-208	196	5	h	h	NOUN
eurjchem-208	196	6	,	,	PUNCT
eurjchem-208	196	7	4.12	4.12	NUM
eurjchem-208	196	8	;	;	PUNCT
eurjchem-208	196	9	n	n	CCONJ
eurjchem-208	196	10	,	,	PUNCT
eurjchem-208	196	11	9.53	9.53	NUM
eurjchem-208	196	12	%	%	NOUN
eurjchem-208	196	13	.	.	PUNCT
eurjchem-208	197	1	2.2.10	2.2.10	NUM
eurjchem-208	197	2	.	.	PUNCT
eurjchem-208	198	1	bis{3‐phenyl‐4‐(4‐phenyl‐2‐thienyl)‐1h‐pyrazol‐1‐	bis{3‐phenyl‐4‐(4‐phenyl‐2‐thienyl)‐1h‐pyrazol‐1‐	ADJ
eurjchem-208	198	2	yl}phosphine	yl}phosphine	DET
eurjchem-208	198	3	oxide	oxide	NOUN
eurjchem-208	198	4	(	(	PUNCT
eurjchem-208	198	5	14	14	NUM
eurjchem-208	198	6	)	)	PUNCT
eurjchem-208	198	7	a	a	DET
eurjchem-208	198	8	mixture	mixture	NOUN
eurjchem-208	198	9	of	of	ADP
eurjchem-208	198	10	bis‐chalcone	bis‐chalcone	NOUN
eurjchem-208	198	11	12	12	NUM
eurjchem-208	198	12	(	(	PUNCT
eurjchem-208	198	13	0.001	0.001	NUM
eurjchem-208	198	14	mol	mol	NOUN
eurjchem-208	198	15	,	,	PUNCT
eurjchem-208	198	16	0.59	0.59	NUM
eurjchem-208	198	17	g	g	NOUN
eurjchem-208	198	18	)	)	PUNCT
eurjchem-208	198	19	and	and	CCONJ
eurjchem-208	198	20	thioglycolic	thioglycolic	ADJ
eurjchem-208	198	21	acid	acid	NOUN
eurjchem-208	198	22	(	(	PUNCT
eurjchem-208	198	23	0.0025	0.0025	NUM
eurjchem-208	198	24	mol	mol	NOUN
eurjchem-208	198	25	,	,	PUNCT
eurjchem-208	198	26	0.23	0.23	NUM
eurjchem-208	198	27	g	g	NOUN
eurjchem-208	198	28	)	)	PUNCT
eurjchem-208	198	29	in	in	ADP
eurjchem-208	198	30	dry	dry	ADJ
eurjchem-208	198	31	dioxane	dioxane	NOUN
eurjchem-208	198	32	(	(	PUNCT
eurjchem-208	198	33	20	20	NUM
eurjchem-208	198	34	cm3	cm3	NOUN
eurjchem-208	198	35	)	)	PUNCT
eurjchem-208	198	36	in	in	ADP
eurjchem-208	198	37	the	the	DET
eurjchem-208	198	38	presence	presence	NOUN
eurjchem-208	198	39	of	of	ADP
eurjchem-208	198	40	anhydrous	anhydrous	ADJ
eurjchem-208	198	41	potassium	potassium	NOUN
eurjchem-208	198	42	carbonate	carbonate	NOUN
eurjchem-208	198	43	(	(	PUNCT
eurjchem-208	198	44	1	1	NUM
eurjchem-208	198	45	g	g	NOUN
eurjchem-208	198	46	)	)	PUNCT
eurjchem-208	198	47	,	,	PUNCT
eurjchem-208	198	48	was	be	AUX
eurjchem-208	198	49	refluxed	refluxe	VERB
eurjchem-208	198	50	for	for	ADP
eurjchem-208	198	51	8	8	NUM
eurjchem-208	198	52	h.	h.	NOUN
eurjchem-208	198	53	the	the	DET
eurjchem-208	198	54	reaction	reaction	NOUN
eurjchem-208	198	55	mixture	mixture	NOUN
eurjchem-208	198	56	was	be	AUX
eurjchem-208	198	57	cooled	cool	VERB
eurjchem-208	198	58	;	;	PUNCT
eurjchem-208	198	59	the	the	DET
eurjchem-208	198	60	resulting	result	VERB
eurjchem-208	198	61	precipitate	precipitate	NOUN
eurjchem-208	198	62	was	be	AUX
eurjchem-208	198	63	filtered	filter	VERB
eurjchem-208	198	64	off	off	ADP
eurjchem-208	198	65	,	,	PUNCT
eurjchem-208	198	66	washed	wash	VERB
eurjchem-208	198	67	with	with	ADP
eurjchem-208	198	68	water	water	NOUN
eurjchem-208	198	69	several	several	ADJ
eurjchem-208	198	70	times	time	NOUN
eurjchem-208	198	71	and	and	CCONJ
eurjchem-208	198	72	crystallized	crystallize	VERB
eurjchem-208	198	73	from	from	ADP
eurjchem-208	198	74	ethanol	ethanol	NOUN
eurjchem-208	198	75	to	to	PART
eurjchem-208	198	76	give	give	VERB
eurjchem-208	198	77	pale	pale	ADJ
eurjchem-208	198	78	yellow	yellow	ADJ
eurjchem-208	198	79	crystals	crystal	NOUN
eurjchem-208	198	80	in	in	ADP
eurjchem-208	198	81	67	67	NUM
eurjchem-208	198	82	%	%	NOUN
eurjchem-208	198	83	yield	yield	NOUN
eurjchem-208	198	84	.	.	PUNCT
eurjchem-208	199	1	m.p	m.p	PROPN
eurjchem-208	199	2	.	.	PROPN
eurjchem-208	199	3	:	:	PUNCT
eurjchem-208	200	1	228–230	228–230	NUM
eurjchem-208	200	2	oc	oc	PROPN
eurjchem-208	200	3	.	.	PROPN
eurjchem-208	200	4	ir	ir	PROPN
eurjchem-208	200	5	(	(	PUNCT
eurjchem-208	200	6	kbr	kbr	PROPN
eurjchem-208	200	7	,	,	PUNCT
eurjchem-208	200	8	max	max	PROPN
eurjchem-208	200	9	,	,	PUNCT
eurjchem-208	200	10	cm‐1	cm‐1	PROPN
eurjchem-208	200	11	):	):	PUNCT
eurjchem-208	200	12	3057	3057	NUM
eurjchem-208	200	13	(	(	PUNCT
eurjchem-208	200	14	c	c	X
eurjchem-208	200	15	–	–	PUNCT
eurjchem-208	200	16	harom	harom	NOUN
eurjchem-208	200	17	)	)	PUNCT
eurjchem-208	200	18	,	,	PUNCT
eurjchem-208	200	19	2363	2363	NUM
eurjchem-208	200	20	(	(	PUNCT
eurjchem-208	200	21	br	br	NOUN
eurjchem-208	200	22	,	,	PUNCT
eurjchem-208	200	23	p	p	NOUN
eurjchem-208	200	24	–	–	PUNCT
eurjchem-208	200	25	h	h	NOUN
eurjchem-208	200	26	)	)	PUNCT
eurjchem-208	200	27	,	,	PUNCT
eurjchem-208	200	28	1614	1614	NUM
eurjchem-208	200	29	(	(	PUNCT
eurjchem-208	200	30	c	c	NOUN
eurjchem-208	200	31	=	=	NOUN
eurjchem-208	200	32	cthiophene	cthiophene	NOUN
eurjchem-208	200	33	)	)	PUNCT
eurjchem-208	200	34	,	,	PUNCT
eurjchem-208	200	35	1597	1597	NUM
eurjchem-208	200	36	(	(	PUNCT
eurjchem-208	200	37	c	c	NOUN
eurjchem-208	200	38	=	=	SYM
eurjchem-208	200	39	n	n	NUM
eurjchem-208	200	40	)	)	PUNCT
eurjchem-208	200	41	,	,	PUNCT
eurjchem-208	200	42	1533	1533	NUM
eurjchem-208	200	43	(	(	PUNCT
eurjchem-208	200	44	c	c	NOUN
eurjchem-208	200	45	=	=	SYM
eurjchem-208	200	46	c	c	NOUN
eurjchem-208	200	47	)	)	PUNCT
eurjchem-208	200	48	,	,	PUNCT
eurjchem-208	200	49	1209	1209	NUM
eurjchem-208	200	50	(	(	PUNCT
eurjchem-208	200	51	p	p	NOUN
eurjchem-208	200	52	=	=	NOUN
eurjchem-208	200	53	o	o	NOUN
eurjchem-208	200	54	)	)	PUNCT
eurjchem-208	200	55	.	.	PUNCT
eurjchem-208	201	1	1h	1h	NUM
eurjchem-208	201	2	nmr	nmr	NOUN
eurjchem-208	201	3	(	(	PUNCT
eurjchem-208	201	4	dmso	dmso	NOUN
eurjchem-208	201	5	,	,	PUNCT
eurjchem-208	201	6	δ	δ	PROPN
eurjchem-208	201	7	ppm	ppm	VERB
eurjchem-208	201	8	):	):	PUNCT
eurjchem-208	201	9	6.60	6.60	NUM
eurjchem-208	201	10	(	(	PUNCT
eurjchem-208	201	11	t	t	PROPN
eurjchem-208	201	12	,	,	PUNCT
eurjchem-208	201	13	2h	2h	NUM
eurjchem-208	201	14	,	,	PUNCT
eurjchem-208	201	15	j=9.2	j=9.2	NOUN
eurjchem-208	201	16	hz	hz	PROPN
eurjchem-208	201	17	,	,	PUNCT
eurjchem-208	201	18	c3	c3	PROPN
eurjchem-208	201	19	–	–	PUNCT
eurjchem-208	201	20	hthiophene	hthiophene	ADJ
eurjchem-208	201	21	)	)	PUNCT
eurjchem-208	201	22	,	,	PUNCT
eurjchem-208	201	23	7.08	7.08	NUM
eurjchem-208	201	24	(	(	PUNCT
eurjchem-208	201	25	d	d	NOUN
eurjchem-208	201	26	,	,	PUNCT
eurjchem-208	201	27	2h	2h	NUM
eurjchem-208	201	28	,	,	PUNCT
eurjchem-208	201	29	j=8.6	j=8.6	PROPN
eurjchem-208	201	30	hz	hz	PROPN
eurjchem-208	201	31	,	,	PUNCT
eurjchem-208	201	32	c5	c5	PROPN
eurjchem-208	201	33	–	–	PUNCT
eurjchem-208	201	34	hthiophene	hthiophene	ADJ
eurjchem-208	201	35	)	)	PUNCT
eurjchem-208	201	36	,	,	PUNCT
eurjchem-208	201	37	7.64	7.64	NUM
eurjchem-208	201	38	(	(	PUNCT
eurjchem-208	201	39	d	d	PROPN
eurjchem-208	201	40	,	,	PUNCT
eurjchem-208	201	41	1h	1h	NUM
eurjchem-208	201	42	,	,	PUNCT
eurjchem-208	201	43	jph=	jph=	PROPN
eurjchem-208	201	44	594	594	NUM
eurjchem-208	201	45	hz	hz	VERB
eurjchem-208	201	46	,	,	PUNCT
eurjchem-208	201	47	p	p	NOUN
eurjchem-208	201	48	–	–	PUNCT
eurjchem-208	201	49	h	h	NOUN
eurjchem-208	201	50	)	)	PUNCT
eurjchem-208	201	51	,	,	PUNCT
eurjchem-208	201	52	8.53	8.53	NUM
eurjchem-208	201	53	,	,	PUNCT
eurjchem-208	201	54	8.68	8.68	NUM
eurjchem-208	201	55	(	(	PUNCT
eurjchem-208	201	56	ss	ss	PROPN
eurjchem-208	201	57	,	,	PUNCT
eurjchem-208	201	58	2h	2h	NUM
eurjchem-208	201	59	,	,	PUNCT
eurjchem-208	201	60	c5	c5	PROPN
eurjchem-208	201	61	–	–	PUNCT
eurjchem-208	201	62	hpyrazole	hpyrazole	NOUN
eurjchem-208	201	63	)	)	PUNCT
eurjchem-208	201	64	,	,	PUNCT
eurjchem-208	201	65	7.75	7.75	NUM
eurjchem-208	201	66	(	(	PUNCT
eurjchem-208	201	67	d	d	PROPN
eurjchem-208	201	68	,	,	PUNCT
eurjchem-208	201	69	2h	2h	NUM
eurjchem-208	201	70	,	,	PUNCT
eurjchem-208	201	71	j=6.2	j=6.2	NOUN
eurjchem-208	201	72	hz	hz	NOUN
eurjchem-208	201	73	,	,	PUNCT
eurjchem-208	201	74	ph	ph	ADJ
eurjchem-208	201	75	–	–	PUNCT
eurjchem-208	201	76	h	h	NOUN
eurjchem-208	201	77	)	)	PUNCT
eurjchem-208	201	78	,	,	PUNCT
eurjchem-208	201	79	8.25	8.25	NUM
eurjchem-208	201	80	(	(	PUNCT
eurjchem-208	201	81	d	d	PROPN
eurjchem-208	201	82	,	,	PUNCT
eurjchem-208	201	83	1h	1h	NUM
eurjchem-208	201	84	,	,	PUNCT
eurjchem-208	201	85	j=8.2	j=8.2	NOUN
eurjchem-208	201	86	hz	hz	NOUN
eurjchem-208	201	87	,	,	PUNCT
eurjchem-208	201	88	ph	ph	ADJ
eurjchem-208	201	89	–	–	PUNCT
eurjchem-208	201	90	h	h	NOUN
eurjchem-208	201	91	)	)	PUNCT
eurjchem-208	201	92	,	,	PUNCT
eurjchem-208	201	93	8.02	8.02	NUM
eurjchem-208	201	94	(	(	PUNCT
eurjchem-208	201	95	d	d	PROPN
eurjchem-208	201	96	,	,	PUNCT
eurjchem-208	201	97	2h	2h	NUM
eurjchem-208	201	98	,	,	PUNCT
eurjchem-208	201	99	j=7.8	j=7.8	NOUN
eurjchem-208	201	100	hz	hz	NOUN
eurjchem-208	201	101	,	,	PUNCT
eurjchem-208	201	102	ph	ph	ADJ
eurjchem-208	201	103	–	–	PUNCT
eurjchem-208	201	104	h	h	NOUN
eurjchem-208	201	105	)	)	PUNCT
eurjchem-208	201	106	,	,	PUNCT
eurjchem-208	201	107	7.36–7.49	7.36–7.49	NUM
eurjchem-208	201	108	(	(	PUNCT
eurjchem-208	201	109	m	m	PROPN
eurjchem-208	201	110	,	,	PUNCT
eurjchem-208	201	111	14h	14h	NUM
eurjchem-208	201	112	,	,	PUNCT
eurjchem-208	201	113	ph	ph	ADJ
eurjchem-208	201	114	–	–	PUNCT
eurjchem-208	201	115	h	h	NOUN
eurjchem-208	201	116	)	)	PUNCT
eurjchem-208	201	117	,	,	PUNCT
eurjchem-208	201	118	7.53	7.53	NUM
eurjchem-208	201	119	(	(	PUNCT
eurjchem-208	201	120	d	d	PROPN
eurjchem-208	201	121	,	,	PUNCT
eurjchem-208	201	122	1h	1h	NUM
eurjchem-208	201	123	,	,	PUNCT
eurjchem-208	201	124	j=6.6	j=6.6	PROPN
eurjchem-208	201	125	hz	hz	PART
eurjchem-208	201	126	,	,	PUNCT
eurjchem-208	201	127	ph	ph	ADJ
eurjchem-208	201	128	–	–	PUNCT
eurjchem-208	201	129	h	h	NOUN
eurjchem-208	201	130	)	)	PUNCT
eurjchem-208	201	131	.	.	PUNCT
eurjchem-208	202	1	anal	anal	PROPN
eurjchem-208	202	2	.	.	PUNCT
eurjchem-208	202	3	calcd	calcd	NOUN
eurjchem-208	202	4	.	.	PUNCT
eurjchem-208	203	1	for	for	ADP
eurjchem-208	203	2	c38h27n4ops2	c38h27n4ops2	PROPN
eurjchem-208	203	3	(	(	PUNCT
eurjchem-208	203	4	650.75	650.75	NUM
eurjchem-208	203	5	):	):	PUNCT
eurjchem-208	203	6	c	c	X
eurjchem-208	203	7	,	,	PUNCT
eurjchem-208	203	8	70.14	70.14	NUM
eurjchem-208	203	9	;	;	PUNCT
eurjchem-208	203	10	h	h	NOUN
eurjchem-208	203	11	,	,	PUNCT
eurjchem-208	203	12	4.18	4.18	NUM
eurjchem-208	203	13	;	;	PUNCT
eurjchem-208	203	14	n	n	CCONJ
eurjchem-208	203	15	,	,	PUNCT
eurjchem-208	203	16	8.61	8.61	NUM
eurjchem-208	203	17	;	;	PUNCT
eurjchem-208	203	18	s	s	X
eurjchem-208	203	19	,	,	PUNCT
eurjchem-208	203	20	9.85	9.85	NUM
eurjchem-208	203	21	.	.	PUNCT
eurjchem-208	203	22	found	find	VERB
eurjchem-208	203	23	:	:	PUNCT
eurjchem-208	204	1	c	c	X
eurjchem-208	204	2	,	,	PUNCT
eurjchem-208	204	3	70.32	70.32	NUM
eurjchem-208	204	4	;	;	PUNCT
eurjchem-208	204	5	h	h	NOUN
eurjchem-208	204	6	,	,	PUNCT
eurjchem-208	204	7	3.93	3.93	NUM
eurjchem-208	204	8	;	;	PUNCT
eurjchem-208	204	9	n	n	CCONJ
eurjchem-208	204	10	,	,	PUNCT
eurjchem-208	204	11	8.42	8.42	NUM
eurjchem-208	204	12	;	;	PUNCT
eurjchem-208	204	13	s	s	X
eurjchem-208	204	14	,	,	PUNCT
eurjchem-208	204	15	9.48	9.48	NUM
eurjchem-208	204	16	%	%	NOUN
eurjchem-208	204	17	.	.	PUNCT
eurjchem-208	205	1	2.2.11	2.2.11	NUM
eurjchem-208	205	2	.	.	PUNCT
eurjchem-208	205	3	bis{4‐[(2‐ethoxy‐2‐oxido‐5‐phenyl‐2,3‐dihydro‐1,2‐	bis{4‐[(2‐ethoxy‐2‐oxido‐5‐phenyl‐2,3‐dihydro‐1,2‐	NOUN
eurjchem-208	205	4	oxaphosphol‐3‐yl]‐3‐phenyl‐1h‐pyrazol‐1‐yl}phosphine	oxaphosphol‐3‐yl]‐3‐phenyl‐1h‐pyrazol‐1‐yl}phosphine	ADJ
eurjchem-208	205	5	oxide	oxide	NOUN
eurjchem-208	205	6	(	(	PUNCT
eurjchem-208	205	7	16	16	NUM
eurjchem-208	205	8	)	)	PUNCT
eurjchem-208	205	9	a	a	DET
eurjchem-208	205	10	mixture	mixture	NOUN
eurjchem-208	205	11	of	of	ADP
eurjchem-208	205	12	bis‐chalcone	bis‐chalcone	NOUN
eurjchem-208	205	13	12	12	NUM
eurjchem-208	205	14	(	(	PUNCT
eurjchem-208	205	15	0.001	0.001	NUM
eurjchem-208	205	16	mol	mol	NOUN
eurjchem-208	205	17	,	,	PUNCT
eurjchem-208	205	18	0.59	0.59	NUM
eurjchem-208	205	19	g	g	NOUN
eurjchem-208	205	20	)	)	PUNCT
eurjchem-208	205	21	and	and	CCONJ
eurjchem-208	205	22	diethyl	diethyl	NOUN
eurjchem-208	205	23	phosphite	phosphite	NOUN
eurjchem-208	205	24	(	(	PUNCT
eurjchem-208	205	25	5	5	NUM
eurjchem-208	205	26	cm3	cm3	NOUN
eurjchem-208	205	27	)	)	PUNCT
eurjchem-208	205	28	in	in	ADP
eurjchem-208	205	29	the	the	DET
eurjchem-208	205	30	presence	presence	NOUN
eurjchem-208	205	31	of	of	ADP
eurjchem-208	205	32	boron	boron	NOUN
eurjchem-208	205	33	trifluorideetherate	trifluorideetherate	NOUN
eurjchem-208	205	34	(	(	PUNCT
eurjchem-208	205	35	0.2	0.2	NUM
eurjchem-208	205	36	cm3	cm3	NOUN
eurjchem-208	205	37	)	)	PUNCT
eurjchem-208	205	38	,	,	PUNCT
eurjchem-208	205	39	was	be	AUX
eurjchem-208	205	40	heated	heat	VERB
eurjchem-208	205	41	on	on	ADP
eurjchem-208	205	42	water	water	NOUN
eurjchem-208	205	43	bath	bath	NOUN
eurjchem-208	205	44	for	for	ADP
eurjchem-208	205	45	8	8	NUM
eurjchem-208	205	46	h.	h.	NOUN
eurjchem-208	205	47	the	the	DET
eurjchem-208	205	48	excess	excess	NOUN
eurjchem-208	205	49	of	of	ADP
eurjchem-208	205	50	diethyl	diethyl	NOUN
eurjchem-208	205	51	phosphite	phosphite	NOUN
eurjchem-208	205	52	was	be	AUX
eurjchem-208	205	53	removed	remove	VERB
eurjchem-208	205	54	under	under	ADP
eurjchem-208	205	55	reduced	reduced	ADJ
eurjchem-208	205	56	pressure	pressure	NOUN
eurjchem-208	205	57	.	.	PUNCT
eurjchem-208	206	1	the	the	DET
eurjchem-208	206	2	formed	form	VERB
eurjchem-208	206	3	precipitate	precipitate	NOUN
eurjchem-208	206	4	was	be	AUX
eurjchem-208	206	5	filtered	filter	VERB
eurjchem-208	206	6	off	off	ADP
eurjchem-208	206	7	and	and	CCONJ
eurjchem-208	206	8	crystallized	crystallize	VERB
eurjchem-208	206	9	from	from	ADP
eurjchem-208	206	10	ethanol	ethanol	NOUN
eurjchem-208	206	11	to	to	PART
eurjchem-208	206	12	give	give	VERB
eurjchem-208	206	13	yellow	yellow	ADJ
eurjchem-208	206	14	crystals	crystal	NOUN
eurjchem-208	206	15	in	in	ADP
eurjchem-208	206	16	82	82	NUM
eurjchem-208	206	17	%	%	NOUN
eurjchem-208	206	18	yield	yield	NOUN
eurjchem-208	206	19	.	.	PUNCT
eurjchem-208	207	1	m.p	m.p	PROPN
eurjchem-208	207	2	.	.	PROPN
eurjchem-208	207	3	:	:	PUNCT
eurjchem-208	208	1	189−191	189−191	NUM
eurjchem-208	208	2	oc	oc	X
eurjchem-208	208	3	.	.	PROPN
eurjchem-208	209	1	ir	ir	PROPN
eurjchem-208	209	2	(	(	PUNCT
eurjchem-208	209	3	kbr	kbr	PROPN
eurjchem-208	209	4	,	,	PUNCT
eurjchem-208	209	5	max	max	PROPN
eurjchem-208	209	6	,	,	PUNCT
eurjchem-208	209	7	cm‐1	cm‐1	NUM
eurjchem-208	209	8	):	):	PUNCT
eurjchem-208	209	9	3059	3059	NUM
eurjchem-208	209	10	(	(	PUNCT
eurjchem-208	209	11	c−harom	c−harom	NOUN
eurjchem-208	209	12	)	)	PUNCT
eurjchem-208	209	13	,	,	PUNCT
eurjchem-208	209	14	2916	2916	NUM
eurjchem-208	209	15	,	,	PUNCT
eurjchem-208	209	16	2895	2895	NUM
eurjchem-208	209	17	(	(	PUNCT
eurjchem-208	209	18	c−haliph	c−haliph	NOUN
eurjchem-208	209	19	)	)	PUNCT
eurjchem-208	209	20	,	,	PUNCT
eurjchem-208	209	21	2613	2613	NUM
eurjchem-208	209	22	(	(	PUNCT
eurjchem-208	209	23	br	br	PROPN
eurjchem-208	209	24	,	,	PUNCT
eurjchem-208	209	25	p	p	NOUN
eurjchem-208	209	26	–	–	PUNCT
eurjchem-208	209	27	h	h	NOUN
eurjchem-208	209	28	)	)	PUNCT
eurjchem-208	209	29	,	,	PUNCT
eurjchem-208	209	30	1592	1592	NUM
eurjchem-208	209	31	(	(	PUNCT
eurjchem-208	209	32	c	c	NOUN
eurjchem-208	209	33	=	=	SYM
eurjchem-208	209	34	n	n	NUM
eurjchem-208	209	35	)	)	PUNCT
eurjchem-208	209	36	,	,	PUNCT
eurjchem-208	209	37	1531(c	1531(c	PROPN
eurjchem-208	209	38	=	=	SYM
eurjchem-208	209	39	c	c	NOUN
eurjchem-208	209	40	)	)	PUNCT
eurjchem-208	209	41	,	,	PUNCT
eurjchem-208	209	42	1286	1286	NUM
eurjchem-208	209	43	,	,	PUNCT
eurjchem-208	209	44	1211	1211	NUM
eurjchem-208	209	45	(	(	PUNCT
eurjchem-208	209	46	p	p	NOUN
eurjchem-208	209	47	=	=	NOUN
eurjchem-208	209	48	o	o	NOUN
eurjchem-208	209	49	)	)	PUNCT
eurjchem-208	209	50	,	,	PUNCT
eurjchem-208	209	51	1064	1064	NUM
eurjchem-208	209	52	,	,	PUNCT
eurjchem-208	209	53	1015	1015	NUM
eurjchem-208	209	54	(	(	PUNCT
eurjchem-208	209	55	p	p	X
eurjchem-208	209	56	–	–	PUNCT
eurjchem-208	209	57	o	o	NOUN
eurjchem-208	209	58	–	–	PUNCT
eurjchem-208	209	59	c	c	NOUN
eurjchem-208	209	60	)	)	PUNCT
eurjchem-208	209	61	.	.	PUNCT
eurjchem-208	210	1	1h	1h	NUM
eurjchem-208	210	2	nmr	nmr	NOUN
eurjchem-208	210	3	(	(	PUNCT
eurjchem-208	210	4	dmso	dmso	NOUN
eurjchem-208	210	5	,	,	PUNCT
eurjchem-208	210	6	δ	δ	PROPN
eurjchem-208	210	7	ppm	ppm	VERB
eurjchem-208	210	8	):	):	PUNCT
eurjchem-208	210	9	1.34	1.34	NUM
eurjchem-208	210	10	(	(	PUNCT
eurjchem-208	210	11	t	t	PROPN
eurjchem-208	210	12	,	,	PUNCT
eurjchem-208	210	13	6h	6h	NUM
eurjchem-208	210	14	,	,	PUNCT
eurjchem-208	210	15	j=7.2	j=7.2	NOUN
eurjchem-208	210	16	hz	hz	VERB
eurjchem-208	210	17	,	,	PUNCT
eurjchem-208	210	18	ch3ch2o	ch3ch2o	NOUN
eurjchem-208	210	19	)	)	PUNCT
eurjchem-208	210	20	,	,	PUNCT
eurjchem-208	210	21	4.35	4.35	NUM
eurjchem-208	210	22	(	(	PUNCT
eurjchem-208	210	23	q	q	NOUN
eurjchem-208	210	24	,	,	PUNCT
eurjchem-208	210	25	4h	4h	NUM
eurjchem-208	210	26	,	,	PUNCT
eurjchem-208	210	27	j=7.2	j=7.2	NOUN
eurjchem-208	210	28	hz	hz	VERB
eurjchem-208	210	29	,	,	PUNCT
eurjchem-208	210	30	ch3ch2o	ch3ch2o	NOUN
eurjchem-208	210	31	)	)	PUNCT
eurjchem-208	210	32	,	,	PUNCT
eurjchem-208	210	33	6.70	6.70	NUM
eurjchem-208	210	34	(	(	PUNCT
eurjchem-208	210	35	d	d	NOUN
eurjchem-208	210	36	,	,	PUNCT
eurjchem-208	210	37	2h	2h	NUM
eurjchem-208	210	38	,	,	PUNCT
eurjchem-208	210	39	j=28	j=28	NOUN
eurjchem-208	210	40	hz	hz	VERB
eurjchem-208	210	41	,	,	PUNCT
eurjchem-208	210	42	ch	ch	NOUN
eurjchem-208	210	43	–	–	PUNCT
eurjchem-208	210	44	p	p	NOUN
eurjchem-208	210	45	)	)	PUNCT
eurjchem-208	210	46	,	,	PUNCT
eurjchem-208	210	47	7.15	7.15	NUM
eurjchem-208	210	48	(	(	PUNCT
eurjchem-208	210	49	d	d	PROPN
eurjchem-208	210	50	,	,	PUNCT
eurjchem-208	210	51	2h	2h	NUM
eurjchem-208	210	52	,	,	PUNCT
eurjchem-208	210	53	j=5	j=5	PROPN
eurjchem-208	210	54	hz	hz	NOUN
eurjchem-208	210	55	,	,	PUNCT
eurjchem-208	210	56	c4	c4	NOUN
eurjchem-208	210	57	–	–	PUNCT
eurjchem-208	210	58	hoxaphosphole	hoxaphosphole	ADJ
eurjchem-208	210	59	)	)	PUNCT
eurjchem-208	210	60	,	,	PUNCT
eurjchem-208	210	61	7.73	7.73	NUM
eurjchem-208	210	62	(	(	PUNCT
eurjchem-208	210	63	d	d	PROPN
eurjchem-208	210	64	,	,	PUNCT
eurjchem-208	210	65	1h	1h	NUM
eurjchem-208	210	66	,	,	PUNCT
eurjchem-208	210	67	jph=612	jph=612	PROPN
eurjchem-208	210	68	hz	hz	VERB
eurjchem-208	210	69	,	,	PUNCT
eurjchem-208	210	70	p	p	NOUN
eurjchem-208	210	71	–	–	PUNCT
eurjchem-208	210	72	h	h	NOUN
eurjchem-208	210	73	)	)	PUNCT
eurjchem-208	210	74	,	,	PUNCT
eurjchem-208	210	75	7.43–8.33	7.43–8.33	NUM
eurjchem-208	210	76	(	(	PUNCT
eurjchem-208	210	77	m	m	PROPN
eurjchem-208	210	78	,	,	PUNCT
eurjchem-208	210	79	20h	20h	NOUN
eurjchem-208	210	80	,	,	PUNCT
eurjchem-208	210	81	ph−h	ph−h	NOUN
eurjchem-208	210	82	)	)	PUNCT
eurjchem-208	210	83	,	,	PUNCT
eurjchem-208	210	84	8.60	8.60	NUM
eurjchem-208	210	85	(	(	PUNCT
eurjchem-208	210	86	s	s	PROPN
eurjchem-208	210	87	,	,	PUNCT
eurjchem-208	210	88	2h	2h	NUM
eurjchem-208	210	89	,	,	PUNCT
eurjchem-208	210	90	c5−hpyrazole).13c	c5−hpyrazole).13c	NOUN
eurjchem-208	210	91	nmr	nmr	NOUN
eurjchem-208	210	92	(	(	PUNCT
eurjchem-208	210	93	dmso	dmso	NOUN
eurjchem-208	210	94	,	,	PUNCT
eurjchem-208	210	95	δ	δ	PROPN
eurjchem-208	210	96	ppm	ppm	VERB
eurjchem-208	210	97	):	):	PUNCT
eurjchem-208	210	98	13.9	13.9	NUM
eurjchem-208	210	99	(	(	PUNCT
eurjchem-208	210	100	ch3ch2o	ch3ch2o	NOUN
eurjchem-208	210	101	)	)	PUNCT
eurjchem-208	210	102	,	,	PUNCT
eurjchem-208	210	103	54.5	54.5	NUM
eurjchem-208	210	104	(	(	PUNCT
eurjchem-208	210	105	d	d	PROPN
eurjchem-208	210	106	,	,	PUNCT
eurjchem-208	210	107	j=168	j=168	PROPN
eurjchem-208	210	108	hz	hz	NOUN
eurjchem-208	210	109	,	,	PUNCT
eurjchem-208	210	110	c3oxaphosphole	c3oxaphosphole	NOUN
eurjchem-208	210	111	)	)	PUNCT
eurjchem-208	210	112	,	,	PUNCT
eurjchem-208	210	113	62.0	62.0	NUM
eurjchem-208	210	114	(	(	PUNCT
eurjchem-208	210	115	ch3ch2o	ch3ch2o	NOUN
eurjchem-208	210	116	)	)	PUNCT
eurjchem-208	210	117	,	,	PUNCT
eurjchem-208	210	118	119.6	119.6	NUM
eurjchem-208	210	119	(	(	PUNCT
eurjchem-208	210	120	c4oxaphosphole	c4oxaphosphole	PROPN
eurjchem-208	210	121	)	)	PUNCT
eurjchem-208	210	122	,	,	PUNCT
eurjchem-208	210	123	120.6	120.6	NUM
eurjchem-208	210	124	(	(	PUNCT
eurjchem-208	210	125	c4pyrazole	c4pyrazole	NOUN
eurjchem-208	210	126	)	)	PUNCT
eurjchem-208	210	127	,	,	PUNCT
eurjchem-208	210	128	126.6–139.1	126.6–139.1	NUM
eurjchem-208	210	129	(	(	PUNCT
eurjchem-208	210	130	phenyl	phenyl	NOUN
eurjchem-208	210	131	carbons	carbon	NOUN
eurjchem-208	210	132	)	)	PUNCT
eurjchem-208	210	133	,	,	PUNCT
eurjchem-208	210	134	145.4	145.4	NUM
eurjchem-208	210	135	(	(	PUNCT
eurjchem-208	210	136	c5pyrazole	c5pyrazole	NOUN
eurjchem-208	210	137	)	)	PUNCT
eurjchem-208	210	138	,	,	PUNCT
eurjchem-208	210	139	154.6	154.6	NUM
eurjchem-208	210	140	(	(	PUNCT
eurjchem-208	210	141	c3	c3	PROPN
eurjchem-208	210	142	pyrazole	pyrazole	PROPN
eurjchem-208	210	143	)	)	PUNCT
eurjchem-208	210	144	,	,	PUNCT
eurjchem-208	210	145	161.8	161.8	NUM
eurjchem-208	210	146	(	(	PUNCT
eurjchem-208	210	147	c5oxaphosphole	c5oxaphosphole	PROPN
eurjchem-208	210	148	)	)	PUNCT
eurjchem-208	210	149	.	.	PUNCT
eurjchem-208	211	1	ms	ms	NOUN
eurjchem-208	211	2	(	(	PUNCT
eurjchem-208	211	3	m	m	PROPN
eurjchem-208	211	4	/	/	SYM
eurjchem-208	211	5	e	e	NOUN
eurjchem-208	211	6	,	,	PUNCT
eurjchem-208	211	7	%	%	INTJ
eurjchem-208	211	8	):	):	PUNCT
eurjchem-208	211	9	778.66	778.66	NUM
eurjchem-208	211	10	(	(	PUNCT
eurjchem-208	211	11	m+	m+	NUM
eurjchem-208	211	12	,	,	PUNCT
eurjchem-208	211	13	not	not	PART
eurjchem-208	211	14	detected	detect	VERB
eurjchem-208	211	15	)	)	PUNCT
eurjchem-208	211	16	,	,	PUNCT
eurjchem-208	211	17	431	431	NUM
eurjchem-208	211	18	(	(	PUNCT
eurjchem-208	211	19	0.1	0.1	NUM
eurjchem-208	211	20	)	)	PUNCT
eurjchem-208	211	21	,	,	PUNCT
eurjchem-208	211	22	311	311	NUM
eurjchem-208	211	23	(	(	PUNCT
eurjchem-208	211	24	2	2	NUM
eurjchem-208	211	25	)	)	PUNCT
eurjchem-208	211	26	,	,	PUNCT
eurjchem-208	211	27	245	245	NUM
eurjchem-208	211	28	(	(	PUNCT
eurjchem-208	211	29	3	3	NUM
eurjchem-208	211	30	)	)	PUNCT
eurjchem-208	211	31	,	,	PUNCT
eurjchem-208	211	32	149	149	NUM
eurjchem-208	211	33	(	(	PUNCT
eurjchem-208	211	34	72	72	NUM
eurjchem-208	211	35	)	)	PUNCT
eurjchem-208	211	36	,	,	PUNCT
eurjchem-208	211	37	97	97	NUM
eurjchem-208	211	38	(	(	PUNCT
eurjchem-208	211	39	9	9	NUM
eurjchem-208	211	40	)	)	PUNCT
eurjchem-208	211	41	,	,	PUNCT
eurjchem-208	211	42	71	71	NUM
eurjchem-208	211	43	(	(	PUNCT
eurjchem-208	211	44	19	19	NUM
eurjchem-208	211	45	)	)	PUNCT
eurjchem-208	211	46	,	,	PUNCT
eurjchem-208	211	47	57	57	NUM
eurjchem-208	211	48	(	(	PUNCT
eurjchem-208	211	49	100	100	NUM
eurjchem-208	211	50	)	)	PUNCT
eurjchem-208	211	51	.	.	PUNCT
eurjchem-208	212	1	anal	anal	PROPN
eurjchem-208	212	2	.	.	PUNCT
eurjchem-208	212	3	calcd	calcd	NOUN
eurjchem-208	212	4	.	.	PUNCT
eurjchem-208	213	1	for	for	SCONJ
eurjchem-208	213	2	c40h37n4o7p3	c40h37n4o7p3	NOUN
eurjchem-208	213	3	(	(	PUNCT
eurjchem-208	213	4	778.66	778.66	NUM
eurjchem-208	213	5	):	):	PUNCT
eurjchem-208	213	6	c	c	X
eurjchem-208	213	7	,	,	PUNCT
eurjchem-208	213	8	61.70	61.70	NUM
eurjchem-208	213	9	;	;	PUNCT
eurjchem-208	213	10	h	h	X
eurjchem-208	213	11	,	,	PUNCT
eurjchem-208	213	12	4.79	4.79	NUM
eurjchem-208	213	13	;	;	PUNCT
eurjchem-208	213	14	n	n	CCONJ
eurjchem-208	213	15	,	,	PUNCT
eurjchem-208	213	16	7.20	7.20	NUM
eurjchem-208	213	17	.	.	PUNCT
eurjchem-208	213	18	found	find	VERB
eurjchem-208	213	19	:	:	PUNCT
eurjchem-208	214	1	c	c	X
eurjchem-208	214	2	,	,	PUNCT
eurjchem-208	214	3	61.29	61.29	NUM
eurjchem-208	214	4	;	;	PUNCT
eurjchem-208	214	5	h	h	NOUN
eurjchem-208	214	6	,	,	PUNCT
eurjchem-208	214	7	4.44	4.44	NUM
eurjchem-208	214	8	;	;	PUNCT
eurjchem-208	214	9	n	n	CCONJ
eurjchem-208	214	10	,	,	PUNCT
eurjchem-208	214	11	6.79	6.79	NUM
eurjchem-208	214	12	%	%	NOUN
eurjchem-208	214	13	.	.	PUNCT
eurjchem-208	215	1	2.2.11	2.2.11	X
eurjchem-208	215	2	.	.	X
eurjchem-208	216	1	bis{3‐(4`‐biphenyl)‐1h‐pyrazole‐4‐carboxaldehyde	bis{3‐(4`‐biphenyl)‐1h‐pyrazole‐4‐carboxaldehyde	PROPN
eurjchem-208	216	2	n4‐phenylthiosemicarbazone}phosphine	n4‐phenylthiosemicarbazone}phosphine	NOUN
eurjchem-208	216	3	oxide	oxide	NOUN
eurjchem-208	216	4	(	(	PUNCT
eurjchem-208	216	5	18	18	NUM
eurjchem-208	216	6	)	)	PUNCT
eurjchem-208	216	7	a	a	DET
eurjchem-208	216	8	mixture	mixture	NOUN
eurjchem-208	216	9	of	of	ADP
eurjchem-208	216	10	bis(4‐formylpyrazolyl)phosphine	bis(4‐formylpyrazolyl)phosphine	PROPN
eurjchem-208	216	11	oxide	oxide	NOUN
eurjchem-208	216	12	4b	4b	X
eurjchem-208	216	13	(	(	PUNCT
eurjchem-208	216	14	0.001	0.001	NUM
eurjchem-208	216	15	mol	mol	NOUN
eurjchem-208	216	16	,	,	PUNCT
eurjchem-208	216	17	0.54	0.54	NUM
eurjchem-208	216	18	g	g	NOUN
eurjchem-208	216	19	)	)	PUNCT
eurjchem-208	216	20	and	and	CCONJ
eurjchem-208	216	21	4‐phenylthiosemicarbazide	4‐phenylthiosemicarbazide	NUM
eurjchem-208	216	22	(	(	PUNCT
eurjchem-208	216	23	17	17	NUM
eurjchem-208	216	24	)	)	PUNCT
eurjchem-208	216	25	(	(	PUNCT
eurjchem-208	216	26	0.002	0.002	NUM
eurjchem-208	216	27	mol	mol	NOUN
eurjchem-208	216	28	,	,	PUNCT
eurjchem-208	216	29	0.33	0.33	NUM
eurjchem-208	216	30	g	g	NOUN
eurjchem-208	216	31	)	)	PUNCT
eurjchem-208	216	32	in	in	ADP
eurjchem-208	216	33	absolute	absolute	ADJ
eurjchem-208	216	34	ethanol	ethanol	NOUN
eurjchem-208	216	35	(	(	PUNCT
eurjchem-208	216	36	10	10	NUM
eurjchem-208	216	37	cm3	cm3	NOUN
eurjchem-208	216	38	)	)	PUNCT
eurjchem-208	216	39	was	be	AUX
eurjchem-208	216	40	refluxed	refluxe	VERB
eurjchem-208	216	41	for	for	ADP
eurjchem-208	216	42	4	4	NUM
eurjchem-208	216	43	h.	h.	NOUN
eurjchem-208	216	44	the	the	DET
eurjchem-208	216	45	product	product	NOUN
eurjchem-208	216	46	was	be	AUX
eurjchem-208	216	47	precipitated	precipitate	VERB
eurjchem-208	216	48	on	on	ADP
eurjchem-208	216	49	heating	heating	NOUN
eurjchem-208	216	50	,	,	PUNCT
eurjchem-208	216	51	filtered	filter	VERB
eurjchem-208	216	52	off	off	ADP
eurjchem-208	216	53	and	and	CCONJ
eurjchem-208	216	54	crystallized	crystallize	VERB
eurjchem-208	216	55	from	from	ADP
eurjchem-208	216	56	dimethylformamide	dimethylformamide	NOUN
eurjchem-208	216	57	to	to	PART
eurjchem-208	216	58	give	give	VERB
eurjchem-208	216	59	orange	orange	ADJ
eurjchem-208	216	60	yellow	yellow	ADJ
eurjchem-208	216	61	crystals	crystal	NOUN
eurjchem-208	216	62	in	in	ADP
eurjchem-208	216	63	45	45	NUM
eurjchem-208	216	64	%	%	NOUN
eurjchem-208	216	65	yield	yield	NOUN
eurjchem-208	216	66	.	.	PUNCT
eurjchem-208	217	1	m.p	m.p	PROPN
eurjchem-208	217	2	.	.	PROPN
eurjchem-208	217	3	:	:	PUNCT
eurjchem-208	218	1	214–216	214–216	NUM
eurjchem-208	218	2	oc	oc	X
eurjchem-208	218	3	.	.	PROPN
eurjchem-208	218	4	ir	ir	PROPN
eurjchem-208	218	5	(	(	PUNCT
eurjchem-208	218	6	kbr	kbr	PROPN
eurjchem-208	218	7	,	,	PUNCT
eurjchem-208	218	8	max	max	PROPN
eurjchem-208	218	9	,	,	PUNCT
eurjchem-208	218	10	cm‐1	cm‐1	PROPN
eurjchem-208	218	11	):	):	PUNCT
eurjchem-208	218	12	3303	3303	NUM
eurjchem-208	218	13	,	,	PUNCT
eurjchem-208	218	14	3127	3127	NUM
eurjchem-208	218	15	(	(	PUNCT
eurjchem-208	218	16	2nh	2nh	PROPN
eurjchem-208	218	17	)	)	PUNCT
eurjchem-208	218	18	,	,	PUNCT
eurjchem-208	218	19	3055	3055	NUM
eurjchem-208	218	20	,	,	PUNCT
eurjchem-208	218	21	3029	3029	NUM
eurjchem-208	218	22	(	(	PUNCT
eurjchem-208	218	23	c	c	NOUN
eurjchem-208	218	24	–	–	PUNCT
eurjchem-208	218	25	harom	harom	NOUN
eurjchem-208	218	26	)	)	PUNCT
eurjchem-208	218	27	,	,	PUNCT
eurjchem-208	218	28	2359	2359	NUM
eurjchem-208	218	29	(	(	PUNCT
eurjchem-208	218	30	br	br	NOUN
eurjchem-208	218	31	,	,	PUNCT
eurjchem-208	218	32	p	p	NOUN
eurjchem-208	218	33	–	–	PUNCT
eurjchem-208	218	34	h	h	NOUN
eurjchem-208	218	35	)	)	PUNCT
eurjchem-208	218	36	,	,	PUNCT
eurjchem-208	218	37	1621	1621	NUM
eurjchem-208	218	38	(	(	PUNCT
eurjchem-208	218	39	c	c	NOUN
eurjchem-208	218	40	=	=	NOUN
eurjchem-208	218	41	nexocyclic	nexocyclic	ADJ
eurjchem-208	218	42	)	)	PUNCT
eurjchem-208	218	43	,	,	PUNCT
eurjchem-208	218	44	1596	1596	NUM
eurjchem-208	218	45	(	(	PUNCT
eurjchem-208	218	46	c	c	NOUN
eurjchem-208	218	47	=	=	NOUN
eurjchem-208	218	48	nendocyclic	nendocyclic	ADJ
eurjchem-208	218	49	)	)	PUNCT
eurjchem-208	218	50	,	,	PUNCT
eurjchem-208	218	51	1539	1539	NUM
eurjchem-208	218	52	(	(	PUNCT
eurjchem-208	218	53	c	c	X
eurjchem-208	218	54	=	=	SYM
eurjchem-208	218	55	c	c	NOUN
eurjchem-208	218	56	)	)	PUNCT
eurjchem-208	218	57	,	,	PUNCT
eurjchem-208	218	58	1260	1260	NUM
eurjchem-208	218	59	(	(	PUNCT
eurjchem-208	218	60	p	p	NOUN
eurjchem-208	218	61	=	=	NOUN
eurjchem-208	218	62	o	o	NOUN
eurjchem-208	218	63	)	)	PUNCT
eurjchem-208	218	64	,	,	PUNCT
eurjchem-208	218	65	1193	1193	NUM
eurjchem-208	218	66	(	(	PUNCT
eurjchem-208	218	67	c	c	NOUN
eurjchem-208	218	68	=	=	SYM
eurjchem-208	218	69	s	s	NOUN
eurjchem-208	218	70	)	)	PUNCT
eurjchem-208	218	71	.	.	PUNCT
eurjchem-208	219	1	1h	1h	NUM
eurjchem-208	219	2	nmr	nmr	NOUN
eurjchem-208	219	3	(	(	PUNCT
eurjchem-208	219	4	dmso	dmso	NOUN
eurjchem-208	219	5	,	,	PUNCT
eurjchem-208	219	6	δ	δ	PROPN
eurjchem-208	219	7	ppm	ppm	VERB
eurjchem-208	219	8	):	):	PUNCT
eurjchem-208	219	9	7.02	7.02	NUM
eurjchem-208	219	10	(	(	PUNCT
eurjchem-208	219	11	d	d	PROPN
eurjchem-208	219	12	,	,	PUNCT
eurjchem-208	219	13	1h	1h	NUM
eurjchem-208	219	14	,	,	PUNCT
eurjchem-208	219	15	jph=532	jph=532	NOUN
eurjchem-208	219	16	hz	hz	VERB
eurjchem-208	219	17	,	,	PUNCT
eurjchem-208	219	18	p	p	NOUN
eurjchem-208	219	19	–	–	PUNCT
eurjchem-208	219	20	h	h	NOUN
eurjchem-208	219	21	)	)	PUNCT
eurjchem-208	219	22	,	,	PUNCT
eurjchem-208	219	23	6.97–7.79	6.97–7.79	NUM
eurjchem-208	219	24	(	(	PUNCT
eurjchem-208	219	25	m	m	PROPN
eurjchem-208	219	26	,	,	PUNCT
eurjchem-208	219	27	28h	28h	NUM
eurjchem-208	219	28	,	,	PUNCT
eurjchem-208	219	29	ar−h	ar−h	NOUN
eurjchem-208	219	30	)	)	PUNCT
eurjchem-208	219	31	,	,	PUNCT
eurjchem-208	219	32	8.40	8.40	NUM
eurjchem-208	219	33	(	(	PUNCT
eurjchem-208	219	34	s	s	PROPN
eurjchem-208	219	35	,	,	PUNCT
eurjchem-208	219	36	2h	2h	NUM
eurjchem-208	219	37	,	,	PUNCT
eurjchem-208	219	38	c5	c5	PROPN
eurjchem-208	219	39	–	–	PUNCT
eurjchem-208	219	40	hpyrazole	hpyrazole	NOUN
eurjchem-208	219	41	)	)	PUNCT
eurjchem-208	219	42	,	,	PUNCT
eurjchem-208	219	43	8.80	8.80	NUM
eurjchem-208	219	44	(	(	PUNCT
eurjchem-208	219	45	s	s	PROPN
eurjchem-208	219	46	,	,	PUNCT
eurjchem-208	219	47	2h	2h	NUM
eurjchem-208	219	48	,	,	PUNCT
eurjchem-208	219	49	ch	ch	NOUN
eurjchem-208	219	50	=	=	NOUN
eurjchem-208	219	51	n	n	CCONJ
eurjchem-208	219	52	)	)	PUNCT
eurjchem-208	219	53	,	,	PUNCT
eurjchem-208	219	54	9.85	9.85	NUM
eurjchem-208	219	55	(	(	PUNCT
eurjchem-208	219	56	s	s	PROPN
eurjchem-208	219	57	,	,	PUNCT
eurjchem-208	219	58	2h	2h	NUM
eurjchem-208	219	59	,	,	PUNCT
eurjchem-208	219	60	nh	nh	PROPN
eurjchem-208	219	61	exchangeable	exchangeable	ADJ
eurjchem-208	219	62	with	with	ADP
eurjchem-208	219	63	d2o	d2o	NOUN
eurjchem-208	219	64	)	)	PUNCT
eurjchem-208	219	65	,	,	PUNCT
eurjchem-208	219	66	11.71	11.71	NUM
eurjchem-208	219	67	(	(	PUNCT
eurjchem-208	219	68	s	s	PROPN
eurjchem-208	219	69	,	,	PUNCT
eurjchem-208	219	70	2h	2h	NUM
eurjchem-208	219	71	,	,	PUNCT
eurjchem-208	219	72	nh	nh	PROPN
eurjchem-208	219	73	exchangeable	exchangeable	ADJ
eurjchem-208	219	74	with	with	ADP
eurjchem-208	219	75	d2o	d2o	NOUN
eurjchem-208	219	76	)	)	PUNCT
eurjchem-208	219	77	.	.	PUNCT
eurjchem-208	220	1	ms	ms	NOUN
eurjchem-208	220	2	(	(	PUNCT
eurjchem-208	220	3	m	m	PROPN
eurjchem-208	220	4	/	/	SYM
eurjchem-208	220	5	e	e	NOUN
eurjchem-208	220	6	,	,	PUNCT
eurjchem-208	220	7	%	%	INTJ
eurjchem-208	220	8	):	):	PUNCT
eurjchem-208	220	9	840	840	NUM
eurjchem-208	220	10	(	(	PUNCT
eurjchem-208	220	11	m+	m+	NUM
eurjchem-208	220	12	,	,	PUNCT
eurjchem-208	220	13	not	not	PART
eurjchem-208	220	14	detected	detect	VERB
eurjchem-208	220	15	)	)	PUNCT
eurjchem-208	220	16	,	,	PUNCT
eurjchem-208	220	17	761	761	NUM
eurjchem-208	220	18	(	(	PUNCT
eurjchem-208	220	19	m+−ph	m+−ph	PROPN
eurjchem-208	220	20	,	,	PUNCT
eurjchem-208	220	21	−2h	−2h	PROPN
eurjchem-208	220	22	,	,	PUNCT
eurjchem-208	220	23	5	5	NUM
eurjchem-208	220	24	%	%	NOUN
eurjchem-208	220	25	)	)	PUNCT
eurjchem-208	220	26	,	,	PUNCT
eurjchem-208	220	27	701	701	NUM
eurjchem-208	220	28	(	(	PUNCT
eurjchem-208	220	29	5	5	NUM
eurjchem-208	220	30	)	)	PUNCT
eurjchem-208	220	31	,	,	PUNCT
eurjchem-208	220	32	570	570	NUM
eurjchem-208	220	33	(	(	PUNCT
eurjchem-208	220	34	5	5	NUM
eurjchem-208	220	35	)	)	PUNCT
eurjchem-208	220	36	,	,	PUNCT
eurjchem-208	220	37	413	413	NUM
eurjchem-208	220	38	(	(	PUNCT
eurjchem-208	220	39	5	5	NUM
eurjchem-208	220	40	)	)	PUNCT
eurjchem-208	220	41	,	,	PUNCT
eurjchem-208	220	42	259	259	NUM
eurjchem-208	220	43	(	(	PUNCT
eurjchem-208	220	44	5	5	NUM
eurjchem-208	220	45	)	)	PUNCT
eurjchem-208	220	46	,	,	PUNCT
eurjchem-208	220	47	153	153	NUM
eurjchem-208	220	48	(	(	PUNCT
eurjchem-208	220	49	10	10	NUM
eurjchem-208	220	50	)	)	PUNCT
eurjchem-208	220	51	,	,	PUNCT
eurjchem-208	220	52	135	135	NUM
eurjchem-208	220	53	(	(	PUNCT
eurjchem-208	220	54	36	36	NUM
eurjchem-208	220	55	)	)	PUNCT
eurjchem-208	220	56	,	,	PUNCT
eurjchem-208	220	57	93	93	NUM
eurjchem-208	220	58	(	(	PUNCT
eurjchem-208	220	59	97	97	NUM
eurjchem-208	220	60	)	)	PUNCT
eurjchem-208	220	61	,	,	PUNCT
eurjchem-208	220	62	77	77	NUM
eurjchem-208	220	63	(	(	PUNCT
eurjchem-208	220	64	76	76	NUM
eurjchem-208	220	65	)	)	PUNCT
eurjchem-208	220	66	,	,	PUNCT
eurjchem-208	220	67	66	66	NUM
eurjchem-208	220	68	(	(	PUNCT
eurjchem-208	220	69	56	56	NUM
eurjchem-208	220	70	)	)	PUNCT
eurjchem-208	220	71	,	,	PUNCT
eurjchem-208	220	72	51	51	NUM
eurjchem-208	220	73	(	(	PUNCT
eurjchem-208	220	74	100	100	NUM
eurjchem-208	220	75	)	)	PUNCT
eurjchem-208	220	76	.	.	PUNCT
eurjchem-208	221	1	anal	anal	PROPN
eurjchem-208	221	2	.	.	PUNCT
eurjchem-208	221	3	calcd	calcd	NOUN
eurjchem-208	221	4	.	.	PUNCT
eurjchem-208	222	1	for	for	ADP
eurjchem-208	222	2	c46h37n10ops2	c46h37n10ops2	PROPN
eurjchem-208	222	3	(	(	PUNCT
eurjchem-208	222	4	840.98	840.98	NUM
eurjchem-208	222	5	):	):	PUNCT
eurjchem-208	222	6	c	c	X
eurjchem-208	222	7	,	,	PUNCT
eurjchem-208	222	8	65.70	65.70	NUM
eurjchem-208	222	9	;	;	PUNCT
eurjchem-208	222	10	h	h	NOUN
eurjchem-208	222	11	,	,	PUNCT
eurjchem-208	222	12	4.43	4.43	NUM
eurjchem-208	222	13	;	;	PUNCT
eurjchem-208	222	14	n	n	CCONJ
eurjchem-208	222	15	,	,	PUNCT
eurjchem-208	222	16	16.66	16.66	NUM
eurjchem-208	222	17	;	;	PUNCT
eurjchem-208	222	18	s	s	X
eurjchem-208	222	19	,	,	PUNCT
eurjchem-208	222	20	7.63	7.63	NUM
eurjchem-208	222	21	.	.	PUNCT
eurjchem-208	222	22	found	find	VERB
eurjchem-208	222	23	:	:	PUNCT
eurjchem-208	223	1	c	c	X
eurjchem-208	223	2	,	,	PUNCT
eurjchem-208	223	3	65.32	65.32	NUM
eurjchem-208	223	4	;	;	PUNCT
eurjchem-208	223	5	h	h	NOUN
eurjchem-208	223	6	,	,	PUNCT
eurjchem-208	223	7	4.21	4.21	NUM
eurjchem-208	223	8	;	;	PUNCT
eurjchem-208	223	9	n	n	CCONJ
eurjchem-208	223	10	,	,	PUNCT
eurjchem-208	223	11	16.31	16.31	NUM
eurjchem-208	223	12	;	;	PUNCT
eurjchem-208	223	13	s	s	X
eurjchem-208	223	14	,	,	PUNCT
eurjchem-208	223	15	7.30	7.30	NUM
eurjchem-208	223	16	%	%	NOUN
eurjchem-208	223	17	.	.	PUNCT
eurjchem-208	224	1	2.2.12	2.2.12	X
eurjchem-208	224	2	.	.	PUNCT
eurjchem-208	225	1	bis{3‐(4`‐biphenyl)‐4‐[(4‐acetyl‐2‐(n‐phenyl	bis{3‐(4`‐biphenyl)‐4‐[(4‐acetyl‐2‐(n‐phenyl	NOUN
eurjchem-208	225	2	acetamido)‐4,5‐dihydro‐1,3,4‐thiadiazol‐5‐yl]‐1h‐pyrazol‐1‐	acetamido)‐4,5‐dihydro‐1,3,4‐thiadiazol‐5‐yl]‐1h‐pyrazol‐1‐	NOUN
eurjchem-208	225	3	yl}phosphine	yl}phosphine	PRON
eurjchem-208	225	4	oxide	oxide	NOUN
eurjchem-208	225	5	(	(	PUNCT
eurjchem-208	225	6	20	20	NUM
eurjchem-208	225	7	)	)	PUNCT
eurjchem-208	225	8	a	a	DET
eurjchem-208	225	9	solution	solution	NOUN
eurjchem-208	225	10	of	of	ADP
eurjchem-208	225	11	bis‐thiosemicarbazone	bis‐thiosemicarbazone	NUM
eurjchem-208	225	12	18	18	NUM
eurjchem-208	225	13	(	(	PUNCT
eurjchem-208	225	14	0.001	0.001	NUM
eurjchem-208	225	15	mol	mol	NOUN
eurjchem-208	225	16	,	,	PUNCT
eurjchem-208	225	17	0.84	0.84	NUM
eurjchem-208	225	18	g	g	NOUN
eurjchem-208	225	19	)	)	PUNCT
eurjchem-208	225	20	in	in	ADP
eurjchem-208	225	21	acetic	acetic	ADJ
eurjchem-208	225	22	anhydride	anhydride	NOUN
eurjchem-208	225	23	(	(	PUNCT
eurjchem-208	225	24	10	10	NUM
eurjchem-208	225	25	cm3	cm3	NOUN
eurjchem-208	225	26	)	)	PUNCT
eurjchem-208	225	27	was	be	AUX
eurjchem-208	225	28	heated	heat	VERB
eurjchem-208	225	29	under	under	ADP
eurjchem-208	225	30	reflux	reflux	NOUN
eurjchem-208	225	31	for	for	ADP
eurjchem-208	225	32	4	4	NUM
eurjchem-208	225	33	h.	h.	NOUN
eurjchem-208	225	34	the	the	DET
eurjchem-208	225	35	excess	excess	NOUN
eurjchem-208	225	36	of	of	ADP
eurjchem-208	225	37	solvent	solvent	NOUN
eurjchem-208	225	38	was	be	AUX
eurjchem-208	225	39	removed	remove	VERB
eurjchem-208	225	40	under	under	ADP
eurjchem-208	225	41	reduced	reduce	VERB
eurjchem-208	225	42	pressure	pressure	NOUN
eurjchem-208	225	43	and	and	CCONJ
eurjchem-208	225	44	the	the	DET
eurjchem-208	225	45	residue	residue	NOUN
eurjchem-208	225	46	was	be	AUX
eurjchem-208	225	47	poured	pour	VERB
eurjchem-208	225	48	on	on	ADP
eurjchem-208	225	49	ice	ice	NOUN
eurjchem-208	225	50	and	and	CCONJ
eurjchem-208	225	51	stirred	stir	VERB
eurjchem-208	225	52	for	for	ADP
eurjchem-208	225	53	10	10	NUM
eurjchem-208	225	54	minutes	minute	NOUN
eurjchem-208	225	55	.	.	PUNCT
eurjchem-208	226	1	the	the	DET
eurjchem-208	226	2	separated	separate	VERB
eurjchem-208	226	3	solid	solid	ADJ
eurjchem-208	226	4	was	be	AUX
eurjchem-208	226	5	filtered	filter	VERB
eurjchem-208	226	6	off	off	ADP
eurjchem-208	226	7	and	and	CCONJ
eurjchem-208	226	8	crystallized	crystallize	VERB
eurjchem-208	226	9	from	from	ADP
eurjchem-208	226	10	ethanol	ethanol	NOUN
eurjchem-208	226	11	to	to	PART
eurjchem-208	226	12	give	give	VERB
eurjchem-208	226	13	deep	deep	ADJ
eurjchem-208	226	14	green	green	ADJ
eurjchem-208	226	15	crystals	crystal	NOUN
eurjchem-208	226	16	in	in	ADP
eurjchem-208	226	17	56	56	NUM
eurjchem-208	226	18	%	%	NOUN
eurjchem-208	226	19	yield	yield	NOUN
eurjchem-208	226	20	.	.	PUNCT
eurjchem-208	227	1	m.p	m.p	PROPN
eurjchem-208	227	2	.	.	PROPN
eurjchem-208	227	3	:	:	PUNCT
eurjchem-208	228	1	124–126	124–126	NUM
eurjchem-208	228	2	oc	oc	PROPN
eurjchem-208	228	3	.	.	PROPN
eurjchem-208	228	4	ir	ir	PROPN
eurjchem-208	228	5	(	(	PUNCT
eurjchem-208	228	6	kbr	kbr	PROPN
eurjchem-208	228	7	,	,	PUNCT
eurjchem-208	228	8	max	max	PROPN
eurjchem-208	228	9	,	,	PUNCT
eurjchem-208	228	10	cm‐1	cm‐1	PROPN
eurjchem-208	228	11	):	):	PUNCT
eurjchem-208	228	12	3056	3056	NUM
eurjchem-208	228	13	,	,	PUNCT
eurjchem-208	228	14	3028	3028	NUM
eurjchem-208	228	15	(	(	PUNCT
eurjchem-208	228	16	c	c	X
eurjchem-208	228	17	–	–	PUNCT
eurjchem-208	228	18	harom	harom	NOUN
eurjchem-208	228	19	)	)	PUNCT
eurjchem-208	228	20	,	,	PUNCT
eurjchem-208	228	21	2930	2930	NUM
eurjchem-208	228	22	(	(	PUNCT
eurjchem-208	228	23	c	c	NOUN
eurjchem-208	228	24	–	–	PUNCT
eurjchem-208	228	25	haliph	haliph	NOUN
eurjchem-208	228	26	)	)	PUNCT
eurjchem-208	228	27	,	,	PUNCT
eurjchem-208	228	28	2361	2361	NUM
eurjchem-208	228	29	(	(	PUNCT
eurjchem-208	228	30	p	p	X
eurjchem-208	228	31	–	–	PUNCT
eurjchem-208	228	32	h	h	NOUN
eurjchem-208	228	33	)	)	PUNCT
eurjchem-208	228	34	,	,	PUNCT
eurjchem-208	228	35	1688	1688	NUM
eurjchem-208	228	36	(	(	PUNCT
eurjchem-208	228	37	c	c	NOUN
eurjchem-208	228	38	=	=	NOUN
eurjchem-208	228	39	o	o	NOUN
eurjchem-208	228	40	)	)	PUNCT
eurjchem-208	228	41	,	,	PUNCT
eurjchem-208	228	42	1667	1667	NUM
eurjchem-208	228	43	(	(	PUNCT
eurjchem-208	228	44	c	c	NOUN
eurjchem-208	228	45	=	=	NOUN
eurjchem-208	228	46	o	o	NOUN
eurjchem-208	228	47	)	)	PUNCT
eurjchem-208	228	48	,	,	PUNCT
eurjchem-208	228	49	1597	1597	NUM
eurjchem-208	228	50	(	(	PUNCT
eurjchem-208	228	51	c	c	NOUN
eurjchem-208	228	52	=	=	SYM
eurjchem-208	228	53	n	n	NUM
eurjchem-208	228	54	)	)	PUNCT
eurjchem-208	228	55	,	,	PUNCT
eurjchem-208	228	56	1540	1540	NUM
eurjchem-208	228	57	(	(	PUNCT
eurjchem-208	228	58	c	c	X
eurjchem-208	228	59	=	=	SYM
eurjchem-208	228	60	c	c	NOUN
eurjchem-208	228	61	)	)	PUNCT
eurjchem-208	228	62	,	,	PUNCT
eurjchem-208	228	63	1297	1297	NUM
eurjchem-208	228	64	(	(	PUNCT
eurjchem-208	228	65	p	p	NOUN
eurjchem-208	228	66	=	=	NOUN
eurjchem-208	228	67	o	o	NOUN
eurjchem-208	228	68	)	)	PUNCT
eurjchem-208	228	69	.	.	PUNCT
eurjchem-208	229	1	1h	1h	NUM
eurjchem-208	229	2	nmr	nmr	NOUN
eurjchem-208	229	3	(	(	PUNCT
eurjchem-208	229	4	dmso	dmso	NOUN
eurjchem-208	229	5	,	,	PUNCT
eurjchem-208	229	6	δ	δ	PROPN
eurjchem-208	229	7	ppm	ppm	VERB
eurjchem-208	229	8	):	):	PUNCT
eurjchem-208	229	9	1.81	1.81	NUM
eurjchem-208	229	10	(	(	PUNCT
eurjchem-208	229	11	s	s	PROPN
eurjchem-208	229	12	,	,	PUNCT
eurjchem-208	229	13	6h	6h	NUM
eurjchem-208	229	14	,	,	PUNCT
eurjchem-208	229	15	ch3	ch3	PROPN
eurjchem-208	229	16	)	)	PUNCT
eurjchem-208	229	17	,	,	PUNCT
eurjchem-208	229	18	1.88	1.88	NUM
eurjchem-208	229	19	(	(	PUNCT
eurjchem-208	229	20	s	s	PROPN
eurjchem-208	229	21	,	,	PUNCT
eurjchem-208	229	22	6h	6h	NUM
eurjchem-208	229	23	,	,	PUNCT
eurjchem-208	229	24	ch3	ch3	PROPN
eurjchem-208	229	25	)	)	PUNCT
eurjchem-208	229	26	,	,	PUNCT
eurjchem-208	229	27	6.30	6.30	NUM
eurjchem-208	229	28	(	(	PUNCT
eurjchem-208	229	29	d	d	PROPN
eurjchem-208	229	30	,	,	PUNCT
eurjchem-208	229	31	1h	1h	NUM
eurjchem-208	229	32	,	,	PUNCT
eurjchem-208	229	33	jph=327	jph=327	PROPN
eurjchem-208	229	34	hz	hz	NOUN
eurjchem-208	229	35	,	,	PUNCT
eurjchem-208	229	36	p	p	NOUN
eurjchem-208	229	37	–	–	PUNCT
eurjchem-208	229	38	h	h	NOUN
eurjchem-208	229	39	)	)	PUNCT
eurjchem-208	229	40	,	,	PUNCT
eurjchem-208	229	41	6.54	6.54	NUM
eurjchem-208	229	42	(	(	PUNCT
eurjchem-208	229	43	brs	brs	PROPN
eurjchem-208	229	44	,	,	PUNCT
eurjchem-208	229	45	2h	2h	NUM
eurjchem-208	229	46	,	,	PUNCT
eurjchem-208	229	47	c5	c5	PROPN
eurjchem-208	229	48	–	–	PUNCT
eurjchem-208	229	49	hthiadiazole	hthiadiazole	NOUN
eurjchem-208	229	50	)	)	PUNCT
eurjchem-208	229	51	,	,	PUNCT
eurjchem-208	229	52	7.35–7.90	7.35–7.90	NUM
eurjchem-208	229	53	(	(	PUNCT
eurjchem-208	229	54	m	m	PROPN
eurjchem-208	229	55	,	,	PUNCT
eurjchem-208	229	56	28h	28h	NUM
eurjchem-208	229	57	,	,	PUNCT
eurjchem-208	229	58	ar−h	ar−h	NOUN
eurjchem-208	229	59	)	)	PUNCT
eurjchem-208	229	60	,	,	PUNCT
eurjchem-208	229	61	8.18	8.18	NUM
eurjchem-208	229	62	(	(	PUNCT
eurjchem-208	229	63	s	s	PROPN
eurjchem-208	229	64	,	,	PUNCT
eurjchem-208	229	65	2h	2h	NUM
eurjchem-208	229	66	,	,	PUNCT
eurjchem-208	229	67	c5	c5	PROPN
eurjchem-208	229	68	–	–	PUNCT
eurjchem-208	229	69	hpyrazole	hpyrazole	NOUN
eurjchem-208	229	70	)	)	PUNCT
eurjchem-208	229	71	.	.	PUNCT
eurjchem-208	230	1	13c	13c	NOUN
eurjchem-208	230	2	nmr	nmr	NOUN
eurjchem-208	230	3	(	(	PUNCT
eurjchem-208	230	4	dmso	dmso	NOUN
eurjchem-208	230	5	,	,	PUNCT
eurjchem-208	230	6	δ	δ	PROPN
eurjchem-208	230	7	ppm	ppm	VERB
eurjchem-208	230	8	):	):	PUNCT
eurjchem-208	230	9	21.0	21.0	NUM
eurjchem-208	230	10	(	(	PUNCT
eurjchem-208	230	11	ch3	ch3	PROPN
eurjchem-208	230	12	)	)	PUNCT
eurjchem-208	230	13	,	,	PUNCT
eurjchem-208	230	14	23.1	23.1	NUM
eurjchem-208	230	15	(	(	PUNCT
eurjchem-208	230	16	ch3	ch3	PROPN
eurjchem-208	230	17	)	)	PUNCT
eurjchem-208	230	18	,	,	PUNCT
eurjchem-208	230	19	60.4	60.4	NUM
eurjchem-208	230	20	(	(	PUNCT
eurjchem-208	230	21	c5thiadiazole	c5thiadiazole	NOUN
eurjchem-208	230	22	)	)	PUNCT
eurjchem-208	230	23	,	,	PUNCT
eurjchem-208	230	24	121.3	121.3	NUM
eurjchem-208	230	25	(	(	PUNCT
eurjchem-208	230	26	c4pyrazole	c4pyrazole	NOUN
eurjchem-208	230	27	)	)	PUNCT
eurjchem-208	230	28	,	,	PUNCT
eurjchem-208	230	29	126.4–140.8	126.4–140.8	NUM
eurjchem-208	230	30	(	(	PUNCT
eurjchem-208	230	31	aromatic	aromatic	ADJ
eurjchem-208	230	32	carbons	carbon	NOUN
eurjchem-208	230	33	)	)	PUNCT
eurjchem-208	230	34	,	,	PUNCT
eurjchem-208	230	35	144.5	144.5	NUM
eurjchem-208	230	36	(	(	PUNCT
eurjchem-208	230	37	c5pyrazole	c5pyrazole	NOUN
eurjchem-208	230	38	)	)	PUNCT
eurjchem-208	230	39	,	,	PUNCT
eurjchem-208	230	40	148.0	148.0	NUM
eurjchem-208	230	41	(	(	PUNCT
eurjchem-208	230	42	c3pyrazole	c3pyrazole	PROPN
eurjchem-208	230	43	)	)	PUNCT
eurjchem-208	230	44	,	,	PUNCT
eurjchem-208	230	45	153.0	153.0	NUM
eurjchem-208	230	46	(	(	PUNCT
eurjchem-208	230	47	c2thiadiazole	c2thiadiazole	NOUN
eurjchem-208	230	48	)	)	PUNCT
eurjchem-208	230	49	,	,	PUNCT
eurjchem-208	230	50	168.0	168.0	NUM
eurjchem-208	230	51	(	(	PUNCT
eurjchem-208	230	52	c	c	NOUN
eurjchem-208	230	53	=	=	NOUN
eurjchem-208	230	54	o	o	NOUN
eurjchem-208	230	55	)	)	PUNCT
eurjchem-208	230	56	,	,	PUNCT
eurjchem-208	230	57	170.1	170.1	NUM
eurjchem-208	230	58	(	(	PUNCT
eurjchem-208	230	59	c	c	NOUN
eurjchem-208	230	60	=	=	NOUN
eurjchem-208	230	61	o	o	NOUN
eurjchem-208	230	62	)	)	PUNCT
eurjchem-208	230	63	.	.	PUNCT
eurjchem-208	231	1	anal	anal	PROPN
eurjchem-208	231	2	.	.	PUNCT
eurjchem-208	231	3	calcd	calcd	NOUN
eurjchem-208	231	4	.	.	PUNCT
eurjchem-208	232	1	for	for	ADP
eurjchem-208	232	2	c54h45n10o5ps2	c54h45n10o5ps2	PROPN
eurjchem-208	232	3	(	(	PUNCT
eurjchem-208	232	4	1009.13	1009.13	NUM
eurjchem-208	232	5	):	):	PUNCT
eurjchem-208	232	6	c	c	X
eurjchem-208	232	7	,	,	PUNCT
eurjchem-208	232	8	64.27	64.27	NUM
eurjchem-208	232	9	;	;	PUNCT
eurjchem-208	232	10	h	h	X
eurjchem-208	232	11	,	,	PUNCT
eurjchem-208	232	12	4.49	4.49	NUM
eurjchem-208	232	13	;	;	PUNCT
eurjchem-208	232	14	n	n	CCONJ
eurjchem-208	232	15	,	,	PUNCT
eurjchem-208	232	16	13.88	13.88	NUM
eurjchem-208	232	17	;	;	PUNCT
eurjchem-208	232	18	s	s	NUM
eurjchem-208	232	19	,	,	PUNCT
eurjchem-208	232	20	6.36	6.36	NUM
eurjchem-208	232	21	.	.	PUNCT
eurjchem-208	232	22	found	find	VERB
eurjchem-208	232	23	:	:	PUNCT
eurjchem-208	233	1	c	c	X
eurjchem-208	233	2	,	,	PUNCT
eurjchem-208	233	3	64.22	64.22	NUM
eurjchem-208	233	4	;	;	PUNCT
eurjchem-208	234	1	h	h	NOUN
eurjchem-208	234	2	,	,	PUNCT
eurjchem-208	234	3	4.31	4.31	NUM
eurjchem-208	234	4	;	;	PUNCT
eurjchem-208	234	5	n	n	CCONJ
eurjchem-208	234	6	,	,	PUNCT
eurjchem-208	234	7	13.28	13.28	NUM
eurjchem-208	234	8	;	;	PUNCT
eurjchem-208	234	9	s	s	X
eurjchem-208	234	10	,	,	PUNCT
eurjchem-208	234	11	6.01	6.01	NUM
eurjchem-208	234	12	%	%	NOUN
eurjchem-208	234	13	.	.	PUNCT
eurjchem-208	235	1	2.2.13	2.2.13	NUM
eurjchem-208	235	2	.	.	PUNCT
eurjchem-208	235	3	bis{3‐(4`‐biphenyl)‐4‐[2‐ethoxy‐6‐phenylamino‐2‐	bis{3‐(4`‐biphenyl)‐4‐[2‐ethoxy‐6‐phenylamino‐2‐	VERB
eurjchem-208	235	4	oxido‐3,4‐dihydro‐2h‐1,4,5,2‐thiadiazaphosphinin‐3‐yl]‐1h‐	oxido‐3,4‐dihydro‐2h‐1,4,5,2‐thiadiazaphosphinin‐3‐yl]‐1h‐	ADP
eurjchem-208	235	5	pyrazol‐1‐yl	pyrazol‐1‐yl	X
eurjchem-208	235	6	]	]	PUNCT
eurjchem-208	235	7	}	}	PUNCT
eurjchem-208	235	8	phosphine	phosphine	ADJ
eurjchem-208	235	9	oxide	oxide	NOUN
eurjchem-208	235	10	(	(	PUNCT
eurjchem-208	235	11	22	22	NUM
eurjchem-208	235	12	)	)	PUNCT
eurjchem-208	235	13	a	a	DET
eurjchem-208	235	14	mixture	mixture	NOUN
eurjchem-208	235	15	of	of	ADP
eurjchem-208	235	16	bis	bis	ADJ
eurjchem-208	235	17	–	–	PUNCT
eurjchem-208	235	18	thiosemicarbazone	thiosemicarbazone	NOUN
eurjchem-208	235	19	18	18	NUM
eurjchem-208	235	20	(	(	PUNCT
eurjchem-208	235	21	0.001	0.001	NUM
eurjchem-208	235	22	mol	mol	NOUN
eurjchem-208	235	23	,	,	PUNCT
eurjchem-208	235	24	0.84	0.84	NUM
eurjchem-208	235	25	g	g	NOUN
eurjchem-208	235	26	)	)	PUNCT
eurjchem-208	235	27	and	and	CCONJ
eurjchem-208	235	28	diethyl	diethyl	NOUN
eurjchem-208	235	29	phosphite	phosphite	NOUN
eurjchem-208	235	30	(	(	PUNCT
eurjchem-208	235	31	8	8	NUM
eurjchem-208	235	32	cm3	cm3	NOUN
eurjchem-208	235	33	)	)	PUNCT
eurjchem-208	235	34	in	in	ADP
eurjchem-208	235	35	the	the	DET
eurjchem-208	235	36	presence	presence	NOUN
eurjchem-208	235	37	of	of	ADP
eurjchem-208	235	38	boron	boron	NOUN
eurjchem-208	235	39	trifluorideetherate	trifluorideetherate	NOUN
eurjchem-208	235	40	(	(	PUNCT
eurjchem-208	235	41	0.2	0.2	NUM
eurjchem-208	235	42	cm3	cm3	NOUN
eurjchem-208	235	43	)	)	PUNCT
eurjchem-208	235	44	,	,	PUNCT
eurjchem-208	235	45	was	be	AUX
eurjchem-208	235	46	heated	heat	VERB
eurjchem-208	235	47	on	on	ADP
eurjchem-208	235	48	water	water	NOUN
eurjchem-208	235	49	bath	bath	NOUN
eurjchem-208	235	50	for	for	ADP
eurjchem-208	235	51	10	10	NUM
eurjchem-208	235	52	h.	h.	NOUN
eurjchem-208	235	53	the	the	DET
eurjchem-208	235	54	excess	excess	NOUN
eurjchem-208	235	55	of	of	ADP
eurjchem-208	235	56	diethyl	diethyl	NOUN
eurjchem-208	235	57	phosphite	phosphite	NOUN
eurjchem-208	235	58	was	be	AUX
eurjchem-208	235	59	removed	remove	VERB
eurjchem-208	235	60	under	under	ADP
eurjchem-208	235	61	reduced	reduced	ADJ
eurjchem-208	235	62	pressure	pressure	NOUN
eurjchem-208	235	63	.	.	PUNCT
eurjchem-208	236	1	the	the	DET
eurjchem-208	236	2	residue	residue	NOUN
eurjchem-208	236	3	was	be	AUX
eurjchem-208	236	4	treated	treat	VERB
eurjchem-208	236	5	with	with	ADP
eurjchem-208	236	6	ethyl	ethyl	PROPN
eurjchem-208	236	7	acetate	acetate	PROPN
eurjchem-208	236	8	to	to	PART
eurjchem-208	236	9	give	give	VERB
eurjchem-208	236	10	solid	solid	ADJ
eurjchem-208	236	11	which	which	PRON
eurjchem-208	236	12	was	be	AUX
eurjchem-208	236	13	filtered	filter	VERB
eurjchem-208	236	14	off	off	ADP
eurjchem-208	236	15	and	and	CCONJ
eurjchem-208	236	16	crystallized	crystallize	VERB
eurjchem-208	236	17	from	from	ADP
eurjchem-208	236	18	ethyl	ethyl	PROPN
eurjchem-208	236	19	acetate	acetate	NOUN
eurjchem-208	236	20	to	to	PART
eurjchem-208	236	21	give	give	VERB
eurjchem-208	236	22	beige	beige	ADJ
eurjchem-208	236	23	crystals	crystal	NOUN
eurjchem-208	236	24	in	in	ADP
eurjchem-208	236	25	51	51	NUM
eurjchem-208	236	26	%	%	NOUN
eurjchem-208	236	27	yield	yield	NOUN
eurjchem-208	236	28	.	.	PUNCT
eurjchem-208	237	1	m.p	m.p	PROPN
eurjchem-208	237	2	.	.	PROPN
eurjchem-208	237	3	:	:	PUNCT
eurjchem-208	238	1	158–160	158–160	NUM
eurjchem-208	238	2	oc	oc	NOUN
eurjchem-208	238	3	.	.	PUNCT
eurjchem-208	238	4	ir	ir	PROPN
eurjchem-208	238	5	(	(	PUNCT
eurjchem-208	238	6	kbr	kbr	PROPN
eurjchem-208	238	7	,	,	PUNCT
eurjchem-208	238	8	max	max	PROPN
eurjchem-208	238	9	,	,	PUNCT
eurjchem-208	238	10	cm‐1	cm‐1	PROPN
eurjchem-208	238	11	):	):	PUNCT
eurjchem-208	238	12	3404	3404	NUM
eurjchem-208	238	13	,	,	PUNCT
eurjchem-208	238	14	3276	3276	NUM
eurjchem-208	238	15	(	(	PUNCT
eurjchem-208	238	16	br	br	NOUN
eurjchem-208	238	17	,	,	PUNCT
eurjchem-208	238	18	2nh	2nh	NOUN
eurjchem-208	238	19	)	)	PUNCT
eurjchem-208	238	20	,	,	PUNCT
eurjchem-208	238	21	3058	3058	NUM
eurjchem-208	238	22	(	(	PUNCT
eurjchem-208	238	23	c	c	X
eurjchem-208	238	24	–	–	PUNCT
eurjchem-208	238	25	harom	harom	NOUN
eurjchem-208	238	26	)	)	PUNCT
eurjchem-208	238	27	,	,	PUNCT
eurjchem-208	238	28	2978	2978	NUM
eurjchem-208	238	29	,	,	PUNCT
eurjchem-208	238	30	2850	2850	NUM
eurjchem-208	238	31	abdel‐aziz	abdel‐aziz	NOUN
eurjchem-208	238	32	et	et	PROPN
eurjchem-208	238	33	al./	al./	ADV
eurjchem-208	238	34	european	european	PROPN
eurjchem-208	238	35	journal	journal	PROPN
eurjchem-208	238	36	of	of	ADP
eurjchem-208	238	37	chemistry	chemistry	NOUN
eurjchem-208	238	38	2	2	NUM
eurjchem-208	238	39	(	(	PUNCT
eurjchem-208	238	40	1	1	NUM
eurjchem-208	238	41	)	)	PUNCT
eurjchem-208	238	42	(	(	PUNCT
eurjchem-208	238	43	2011	2011	NUM
eurjchem-208	238	44	)	)	PUNCT
eurjchem-208	238	45	25‐35	25‐35	NUM
eurjchem-208	238	46	29	29	NUM
eurjchem-208	238	47	(	(	PUNCT
eurjchem-208	238	48	c	c	NOUN
eurjchem-208	238	49	–	–	PUNCT
eurjchem-208	238	50	haliph	haliph	NOUN
eurjchem-208	238	51	)	)	PUNCT
eurjchem-208	238	52	,	,	PUNCT
eurjchem-208	238	53	2493	2493	NUM
eurjchem-208	238	54	(	(	PUNCT
eurjchem-208	238	55	p	p	X
eurjchem-208	238	56	–	–	PUNCT
eurjchem-208	238	57	h	h	NOUN
eurjchem-208	238	58	)	)	PUNCT
eurjchem-208	238	59	,	,	PUNCT
eurjchem-208	238	60	1600	1600	NUM
eurjchem-208	238	61	(	(	PUNCT
eurjchem-208	238	62	c	c	NOUN
eurjchem-208	238	63	=	=	SYM
eurjchem-208	238	64	n	n	NUM
eurjchem-208	238	65	)	)	PUNCT
eurjchem-208	238	66	,	,	PUNCT
eurjchem-208	238	67	1543	1543	NUM
eurjchem-208	238	68	(	(	PUNCT
eurjchem-208	238	69	c	c	NOUN
eurjchem-208	238	70	=	=	SYM
eurjchem-208	238	71	c	c	NOUN
eurjchem-208	238	72	)	)	PUNCT
eurjchem-208	238	73	,	,	PUNCT
eurjchem-208	238	74	1228	1228	NUM
eurjchem-208	238	75	,	,	PUNCT
eurjchem-208	238	76	1248	1248	NUM
eurjchem-208	238	77	(	(	PUNCT
eurjchem-208	238	78	2p	2p	NUM
eurjchem-208	238	79	=	=	SYM
eurjchem-208	238	80	o	o	NOUN
eurjchem-208	238	81	)	)	PUNCT
eurjchem-208	238	82	,	,	PUNCT
eurjchem-208	238	83	1046	1046	NUM
eurjchem-208	238	84	(	(	PUNCT
eurjchem-208	238	85	p	p	X
eurjchem-208	238	86	–	–	PUNCT
eurjchem-208	238	87	o	o	NOUN
eurjchem-208	238	88	–	–	PUNCT
eurjchem-208	238	89	c	c	NOUN
eurjchem-208	238	90	)	)	PUNCT
eurjchem-208	238	91	.	.	PUNCT
eurjchem-208	239	1	1h	1h	NUM
eurjchem-208	239	2	nmr	nmr	NOUN
eurjchem-208	239	3	(	(	PUNCT
eurjchem-208	239	4	dmso	dmso	NOUN
eurjchem-208	239	5	,	,	PUNCT
eurjchem-208	239	6	δ	δ	PROPN
eurjchem-208	239	7	ppm	ppm	VERB
eurjchem-208	239	8	):	):	PUNCT
eurjchem-208	239	9	1.16	1.16	NUM
eurjchem-208	239	10	(	(	PUNCT
eurjchem-208	239	11	t	t	PROPN
eurjchem-208	239	12	,	,	PUNCT
eurjchem-208	239	13	6h	6h	NUM
eurjchem-208	239	14	,	,	PUNCT
eurjchem-208	239	15	j=8.2	j=8.2	NOUN
eurjchem-208	239	16	hz	hz	VERB
eurjchem-208	239	17	,	,	PUNCT
eurjchem-208	239	18	ch3ch2o	ch3ch2o	NOUN
eurjchem-208	239	19	)	)	PUNCT
eurjchem-208	239	20	,	,	PUNCT
eurjchem-208	239	21	3.96	3.96	NUM
eurjchem-208	239	22	(	(	PUNCT
eurjchem-208	239	23	q	q	NOUN
eurjchem-208	239	24	,	,	PUNCT
eurjchem-208	239	25	4h	4h	NUM
eurjchem-208	239	26	,	,	PUNCT
eurjchem-208	239	27	j=8.2	j=8.2	NOUN
eurjchem-208	239	28	hz	hz	VERB
eurjchem-208	239	29	,	,	PUNCT
eurjchem-208	239	30	ch3ch2o	ch3ch2o	NOUN
eurjchem-208	239	31	)	)	PUNCT
eurjchem-208	239	32	,	,	PUNCT
eurjchem-208	239	33	4.90	4.90	NUM
eurjchem-208	239	34	(	(	PUNCT
eurjchem-208	239	35	d	d	NOUN
eurjchem-208	239	36	,	,	PUNCT
eurjchem-208	239	37	2h	2h	NUM
eurjchem-208	239	38	,	,	PUNCT
eurjchem-208	239	39	j=20.4	j=20.4	PROPN
eurjchem-208	239	40	hz	hz	NOUN
eurjchem-208	239	41	,	,	PUNCT
eurjchem-208	239	42	c3	c3	PROPN
eurjchem-208	239	43	–	–	PUNCT
eurjchem-208	239	44	hthiadiazaphosphinine	hthiadiazaphosphinine	NOUN
eurjchem-208	239	45	)	)	PUNCT
eurjchem-208	239	46	,	,	PUNCT
eurjchem-208	239	47	6.59–7.79	6.59–7.79	NUM
eurjchem-208	239	48	(	(	PUNCT
eurjchem-208	239	49	m	m	PROPN
eurjchem-208	239	50	,	,	PUNCT
eurjchem-208	239	51	28h	28h	NUM
eurjchem-208	239	52	,	,	PUNCT
eurjchem-208	239	53	ar−h	ar−h	NOUN
eurjchem-208	239	54	)	)	PUNCT
eurjchem-208	239	55	,	,	PUNCT
eurjchem-208	239	56	7.08	7.08	NUM
eurjchem-208	239	57	(	(	PUNCT
eurjchem-208	239	58	d	d	PROPN
eurjchem-208	239	59	,	,	PUNCT
eurjchem-208	239	60	1h	1h	NUM
eurjchem-208	239	61	,	,	PUNCT
eurjchem-208	239	62	jph=532.4	jph=532.4	PROPN
eurjchem-208	239	63	hz	hz	VERB
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eurjchem-208	239	65	p	p	NOUN
eurjchem-208	239	66	–	–	PUNCT
eurjchem-208	239	67	h	h	NOUN
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eurjchem-208	239	69	,	,	PUNCT
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eurjchem-208	239	72	s	s	PROPN
eurjchem-208	239	73	,	,	PUNCT
eurjchem-208	239	74	2h	2h	NUM
eurjchem-208	239	75	,	,	PUNCT
eurjchem-208	239	76	c5	c5	PROPN
eurjchem-208	239	77	–	–	PUNCT
eurjchem-208	239	78	hpyrazole	hpyrazole	NOUN
eurjchem-208	239	79	)	)	PUNCT
eurjchem-208	239	80	,	,	PUNCT
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eurjchem-208	239	84	,	,	PUNCT
eurjchem-208	239	85	2h	2h	NUM
eurjchem-208	239	86	,	,	PUNCT
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eurjchem-208	239	89	with	with	ADP
eurjchem-208	239	90	d2o	d2o	NOUN
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eurjchem-208	239	92	,	,	PUNCT
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eurjchem-208	239	98	,	,	PUNCT
eurjchem-208	239	99	nh	nh	PROPN
eurjchem-208	239	100	exchangeable	exchangeable	ADJ
eurjchem-208	239	101	with	with	ADP
eurjchem-208	239	102	d2o	d2o	NOUN
eurjchem-208	239	103	)	)	PUNCT
eurjchem-208	239	104	.	.	PUNCT
eurjchem-208	240	1	31p	31p	NUM
eurjchem-208	240	2	nmr	nmr	NOUN
eurjchem-208	240	3	(	(	PUNCT
eurjchem-208	240	4	dmso	dmso	NOUN
eurjchem-208	240	5	,	,	PUNCT
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eurjchem-208	240	8	):	):	PUNCT
eurjchem-208	240	9	6.6	6.6	NUM
eurjchem-208	240	10	(	(	PUNCT
eurjchem-208	240	11	o	o	NOUN
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eurjchem-208	240	13	p	p	NOUN
eurjchem-208	240	14	–	–	PUNCT
eurjchem-208	240	15	h	h	NOUN
eurjchem-208	240	16	)	)	PUNCT
eurjchem-208	240	17	,	,	PUNCT
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eurjchem-208	240	19	(	(	PUNCT
eurjchem-208	240	20	eto	eto	PROPN
eurjchem-208	240	21	–	–	PUNCT
eurjchem-208	240	22	p	p	X
eurjchem-208	240	23	=	=	NOUN
eurjchem-208	240	24	o	o	NOUN
eurjchem-208	240	25	)	)	PUNCT
eurjchem-208	240	26	.	.	PUNCT
eurjchem-208	241	1	anal	anal	PROPN
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eurjchem-208	241	3	calcd	calcd	NOUN
eurjchem-208	241	4	.	.	PUNCT
eurjchem-208	242	1	for	for	ADP
eurjchem-208	242	2	c50h47n10o5p3s2	c50h47n10o5p3s2	PROPN
eurjchem-208	242	3	(	(	PUNCT
eurjchem-208	242	4	1025.05	1025.05	NUM
eurjchem-208	242	5	):	):	PUNCT
eurjchem-208	242	6	c	c	NOUN
eurjchem-208	242	7	,	,	PUNCT
eurjchem-208	242	8	58.59	58.59	NUM
eurjchem-208	242	9	;	;	PUNCT
eurjchem-208	242	10	h	h	NOUN
eurjchem-208	242	11	,	,	PUNCT
eurjchem-208	242	12	4.62	4.62	NUM
eurjchem-208	242	13	;	;	PUNCT
eurjchem-208	242	14	n	n	CCONJ
eurjchem-208	242	15	,	,	PUNCT
eurjchem-208	242	16	13.66	13.66	NUM
eurjchem-208	242	17	;	;	PUNCT
eurjchem-208	242	18	s	s	NOUN
eurjchem-208	242	19	,	,	PUNCT
eurjchem-208	242	20	6.26	6.26	NUM
eurjchem-208	242	21	.	.	PUNCT
eurjchem-208	242	22	found	find	VERB
eurjchem-208	242	23	:	:	PUNCT
eurjchem-208	243	1	c	c	X
eurjchem-208	243	2	,	,	PUNCT
eurjchem-208	243	3	58.32	58.32	NUM
eurjchem-208	243	4	;	;	PUNCT
eurjchem-208	243	5	h	h	NOUN
eurjchem-208	243	6	,	,	PUNCT
eurjchem-208	243	7	4.34	4.34	NUM
eurjchem-208	243	8	;	;	PUNCT
eurjchem-208	243	9	n	n	CCONJ
eurjchem-208	243	10	,	,	PUNCT
eurjchem-208	243	11	13.44	13.44	NUM
eurjchem-208	243	12	;	;	PUNCT
eurjchem-208	243	13	s	s	X
eurjchem-208	243	14	,	,	PUNCT
eurjchem-208	243	15	5.94	5.94	NUM
eurjchem-208	243	16	%	%	NOUN
eurjchem-208	243	17	.	.	PUNCT
eurjchem-208	244	1	3	3	X
eurjchem-208	244	2	.	.	NOUN
eurjchem-208	244	3	results	result	NOUN
eurjchem-208	244	4	and	and	CCONJ
eurjchem-208	244	5	discussion	discussion	NOUN
eurjchem-208	244	6	3.1	3.1	NUM
eurjchem-208	244	7	.	.	PUNCT
eurjchem-208	245	1	synthesis	synthesis	VERB
eurjchem-208	245	2	the	the	DET
eurjchem-208	245	3	key	key	ADJ
eurjchem-208	245	4	intermediate	intermediate	NOUN
eurjchem-208	245	5	in	in	ADP
eurjchem-208	245	6	the	the	DET
eurjchem-208	245	7	present	present	ADJ
eurjchem-208	245	8	work	work	NOUN
eurjchem-208	245	9	is	be	AUX
eurjchem-208	245	10	phosphonicdihydrazide	phosphonicdihydrazide	ADJ
eurjchem-208	245	11	(	(	PUNCT
eurjchem-208	245	12	1	1	NUM
eurjchem-208	245	13	)	)	PUNCT
eurjchem-208	245	14	,	,	PUNCT
eurjchem-208	245	15	which	which	PRON
eurjchem-208	245	16	was	be	AUX
eurjchem-208	245	17	obtained	obtain	VERB
eurjchem-208	245	18	from	from	ADP
eurjchem-208	245	19	fusion	fusion	NOUN
eurjchem-208	245	20	of	of	ADP
eurjchem-208	245	21	diethyl	diethyl	NOUN
eurjchem-208	245	22	phosphite	phosphite	NOUN
eurjchem-208	245	23	with	with	ADP
eurjchem-208	245	24	two	two	NUM
eurjchem-208	245	25	equivalent	equivalent	ADJ
eurjchem-208	245	26	amounts	amount	NOUN
eurjchem-208	245	27	of	of	ADP
eurjchem-208	245	28	hydrazine	hydrazine	NOUN
eurjchem-208	245	29	hydrate	hydrate	NOUN
eurjchem-208	245	30	at	at	ADP
eurjchem-208	245	31	70−80	70−80	NUM
eurjchem-208	245	32	oc	oc	ADP
eurjchem-208	245	33	[	[	X
eurjchem-208	245	34	23	23	NUM
eurjchem-208	245	35	]	]	PUNCT
eurjchem-208	245	36	(	(	PUNCT
eurjchem-208	245	37	scheme	scheme	NOUN
eurjchem-208	245	38	1	1	NUM
eurjchem-208	245	39	)	)	PUNCT
eurjchem-208	245	40	.	.	PUNCT
eurjchem-208	246	1	condensation	condensation	NOUN
eurjchem-208	246	2	of	of	ADP
eurjchem-208	246	3	phosphonicdihydrazide	phosphonicdihydrazide	NOUN
eurjchem-208	246	4	(	(	PUNCT
eurjchem-208	246	5	1	1	NUM
eurjchem-208	246	6	)	)	PUNCT
eurjchem-208	246	7	with	with	ADP
eurjchem-208	246	8	acetophenone	acetophenone	NOUN
eurjchem-208	246	9	derivatives	derivative	NOUN
eurjchem-208	246	10	2a‐	2a‐	NUM
eurjchem-208	247	1	d	d	PRON
eurjchem-208	247	2	gave	give	VERB
eurjchem-208	247	3	the	the	DET
eurjchem-208	247	4	corresponding	correspond	VERB
eurjchem-208	247	5	phosphonicdihydrazones	phosphonicdihydrazone	NOUN
eurjchem-208	247	6	3a‐d	3a‐d	ADV
eurjchem-208	247	7	(	(	PUNCT
eurjchem-208	247	8	scheme	scheme	NOUN
eurjchem-208	247	9	1	1	NUM
eurjchem-208	247	10	)	)	PUNCT
eurjchem-208	247	11	.	.	PUNCT
eurjchem-208	248	1	these	these	DET
eurjchem-208	248	2	reactions	reaction	NOUN
eurjchem-208	248	3	were	be	AUX
eurjchem-208	248	4	carried	carry	VERB
eurjchem-208	248	5	out	out	ADP
eurjchem-208	248	6	in	in	ADP
eurjchem-208	248	7	absolute	absolute	ADJ
eurjchem-208	248	8	ethanol	ethanol	NOUN
eurjchem-208	248	9	under	under	ADP
eurjchem-208	248	10	mild	mild	ADJ
eurjchem-208	248	11	conditions	condition	NOUN
eurjchem-208	248	12	,	,	PUNCT
eurjchem-208	248	13	and	and	CCONJ
eurjchem-208	248	14	the	the	DET
eurjchem-208	248	15	products	product	NOUN
eurjchem-208	248	16	were	be	AUX
eurjchem-208	248	17	isolated	isolate	VERB
eurjchem-208	248	18	as	as	ADP
eurjchem-208	248	19	yellow	yellow	ADJ
eurjchem-208	248	20	crystalline	crystalline	NOUN
eurjchem-208	248	21	substances	substance	NOUN
eurjchem-208	248	22	in	in	ADP
eurjchem-208	248	23	46‐71	46‐71	ADJ
eurjchem-208	248	24	%	%	NOUN
eurjchem-208	248	25	yields	yield	NOUN
eurjchem-208	248	26	.	.	PUNCT
eurjchem-208	249	1	structures	structure	NOUN
eurjchem-208	249	2	of	of	ADP
eurjchem-208	249	3	3a‐d	3a‐d	NOUN
eurjchem-208	249	4	were	be	AUX
eurjchem-208	249	5	deduced	deduce	VERB
eurjchem-208	249	6	from	from	ADP
eurjchem-208	249	7	their	their	PRON
eurjchem-208	249	8	spectroscopic	spectroscopic	ADJ
eurjchem-208	249	9	measurements	measurement	NOUN
eurjchem-208	249	10	.	.	PUNCT
eurjchem-208	250	1	the	the	DET
eurjchem-208	250	2	1h	1h	NUM
eurjchem-208	250	3	nmr	nmr	NOUN
eurjchem-208	250	4	spectra	spectra	NOUN
eurjchem-208	250	5	of	of	ADP
eurjchem-208	250	6	compounds	compound	NOUN
eurjchem-208	250	7	3a‐d	3a‐d	ADP
eurjchem-208	250	8	recorded	record	VERB
eurjchem-208	250	9	signals	signal	NOUN
eurjchem-208	250	10	of	of	ADP
eurjchem-208	250	11	methyl	methyl	NOUN
eurjchem-208	250	12	protons	proton	NOUN
eurjchem-208	250	13	in	in	ADP
eurjchem-208	250	14	the	the	DET
eurjchem-208	250	15	region	region	NOUN
eurjchem-208	250	16			PROPN
eurjchem-208	250	17	2.07−2.28	2.07−2.28	PROPN
eurjchem-208	250	18	ppm	ppm	NOUN
eurjchem-208	250	19	.	.	PUNCT
eurjchem-208	251	1	also	also	ADV
eurjchem-208	251	2	,	,	PUNCT
eurjchem-208	251	3	the	the	DET
eurjchem-208	251	4	signals	signal	NOUN
eurjchem-208	251	5	of	of	ADP
eurjchem-208	251	6	nh	nh	PROPN
eurjchem-208	251	7	and	and	CCONJ
eurjchem-208	251	8	h−p	h−p	NUM
eurjchem-208	251	9	=	=	NOUN
eurjchem-208	251	10	o	o	NOUN
eurjchem-208	251	11	protons	proton	NOUN
eurjchem-208	251	12	were	be	AUX
eurjchem-208	251	13	displaced	displace	VERB
eurjchem-208	251	14	,	,	PUNCT
eurjchem-208	251	15	presumably	presumably	ADV
eurjchem-208	251	16	as	as	ADP
eurjchem-208	251	17	a	a	DET
eurjchem-208	251	18	result	result	NOUN
eurjchem-208	251	19	of	of	ADP
eurjchem-208	251	20	rapid	rapid	ADJ
eurjchem-208	251	21	protons	proton	NOUN
eurjchem-208	251	22	exchange	exchange	NOUN
eurjchem-208	251	23	in	in	ADP
eurjchem-208	251	24	two	two	NUM
eurjchem-208	251	25	types	type	NOUN
eurjchem-208	251	26	of	of	ADP
eurjchem-208	251	27	tautomeric	tautomeric	ADJ
eurjchem-208	251	28	equilibriums	equilibrium	NOUN
eurjchem-208	251	29	.	.	PUNCT
eurjchem-208	252	1	the	the	DET
eurjchem-208	252	2	first	first	ADJ
eurjchem-208	252	3	type	type	NOUN
eurjchem-208	252	4	is	be	AUX
eurjchem-208	252	5	tautomeric	tautomeric	ADJ
eurjchem-208	252	6	amide‐imide	amide‐imide	NOUN
eurjchem-208	252	7	equilibrium	equilibrium	NOUN
eurjchem-208	252	8	(	(	PUNCT
eurjchem-208	252	9	i	i	PROPN
eurjchem-208	252	10	,	,	PUNCT
eurjchem-208	252	11	ii	ii	PROPN
eurjchem-208	252	12	,	,	PUNCT
eurjchem-208	252	13	iii	iii	PROPN
eurjchem-208	252	14	)	)	PUNCT
eurjchem-208	252	15	,	,	PUNCT
eurjchem-208	252	16	while	while	SCONJ
eurjchem-208	252	17	in	in	ADP
eurjchem-208	252	18	the	the	DET
eurjchem-208	252	19	second	second	ADJ
eurjchem-208	252	20	type	type	NOUN
eurjchem-208	252	21	,	,	PUNCT
eurjchem-208	252	22	hydrophosphoryl	hydrophosphoryl	ADJ
eurjchem-208	252	23	unit	unit	NOUN
eurjchem-208	252	24	in	in	ADP
eurjchem-208	252	25	solutions	solution	NOUN
eurjchem-208	252	26	easily	easily	ADV
eurjchem-208	252	27	undergoes	undergo	VERB
eurjchem-208	252	28	the	the	DET
eurjchem-208	252	29	tautomeric	tautomeric	ADJ
eurjchem-208	252	30	transition	transition	NOUN
eurjchem-208	252	31	,	,	PUNCT
eurjchem-208	252	32	providing	provide	VERB
eurjchem-208	252	33	it	it	PRON
eurjchem-208	252	34	a	a	DET
eurjchem-208	252	35	unique	unique	ADJ
eurjchem-208	252	36	combination	combination	NOUN
eurjchem-208	252	37	of	of	ADP
eurjchem-208	252	38	properties	property	NOUN
eurjchem-208	252	39	of	of	ADP
eurjchem-208	252	40	pentavalent	pentavalent	NOUN
eurjchem-208	252	41	(	(	PUNCT
eurjchem-208	252	42	λ5	λ5	NOUN
eurjchem-208	252	43	,	,	PUNCT
eurjchem-208	252	44	σ4	σ4	NOUN
eurjchem-208	252	45	form	form	NOUN
eurjchem-208	252	46	)	)	PUNCT
eurjchem-208	252	47	and	and	CCONJ
eurjchem-208	252	48	trivalent	trivalent	NOUN
eurjchem-208	252	49	(	(	PUNCT
eurjchem-208	252	50	λ3	λ3	PROPN
eurjchem-208	252	51	,	,	PUNCT
eurjchem-208	252	52	σ3	σ3	NOUN
eurjchem-208	252	53	form	form	NOUN
eurjchem-208	252	54	)	)	PUNCT
eurjchem-208	252	55	phosphorus	phosphorus	NOUN
eurjchem-208	252	56	atom	atom	NOUN
eurjchem-208	252	57	(	(	PUNCT
eurjchem-208	252	58	phosphonate	phosphonate	NOUN
eurjchem-208	252	59	–	–	PUNCT
eurjchem-208	252	60	phosphite	phosphite	NOUN
eurjchem-208	252	61	i	i	PRON
eurjchem-208	252	62	and	and	CCONJ
eurjchem-208	252	63	iv	iv	X
eurjchem-208	252	64	)	)	PUNCT
eurjchem-208	252	65	(	(	PUNCT
eurjchem-208	252	66	scheme	scheme	NOUN
eurjchem-208	252	67	2	2	NUM
eurjchem-208	252	68	)	)	PUNCT
eurjchem-208	252	69	[	[	X
eurjchem-208	252	70	24‐27	24‐27	NUM
eurjchem-208	252	71	]	]	X
eurjchem-208	252	72	.	.	PUNCT
eurjchem-208	253	1	also	also	ADV
eurjchem-208	253	2	,	,	PUNCT
eurjchem-208	253	3	the	the	DET
eurjchem-208	253	4	13c	13c	NOUN
eurjchem-208	253	5	nmr	nmr	NOUN
eurjchem-208	253	6	spectrum	spectrum	NOUN
eurjchem-208	253	7	of	of	ADP
eurjchem-208	253	8	compound	compound	NOUN
eurjchem-208	253	9	3a	3a	NUM
eurjchem-208	253	10	displayed	display	VERB
eurjchem-208	253	11	the	the	DET
eurjchem-208	253	12	carbon	carbon	NOUN
eurjchem-208	253	13	atoms	atom	NOUN
eurjchem-208	253	14	of	of	ADP
eurjchem-208	253	15	methyl	methyl	NOUN
eurjchem-208	253	16	and	and	CCONJ
eurjchem-208	253	17	c	c	NOUN
eurjchem-208	253	18	=	=	NOUN
eurjchem-208	253	19	n	n	PRON
eurjchem-208	253	20	groups	group	NOUN
eurjchem-208	253	21	at	at	ADP
eurjchem-208	253	22			NUM
eurjchem-208	253	23	14.7	14.7	NUM
eurjchem-208	253	24	and	and	CCONJ
eurjchem-208	253	25	157.2	157.2	NUM
eurjchem-208	253	26	ppm	ppm	NOUN
eurjchem-208	253	27	,	,	PUNCT
eurjchem-208	253	28	respectively	respectively	ADV
eurjchem-208	253	29	.	.	PUNCT
eurjchem-208	254	1	furthermore	furthermore	ADV
eurjchem-208	254	2	,	,	PUNCT
eurjchem-208	254	3	compound	compound	VERB
eurjchem-208	254	4	3c	3c	NUM
eurjchem-208	254	5	exhibited	exhibit	VERB
eurjchem-208	254	6	a	a	DET
eurjchem-208	254	7	signal	signal	NOUN
eurjchem-208	254	8	in	in	ADP
eurjchem-208	254	9	its	its	PRON
eurjchem-208	254	10	31p	31p	NUM
eurjchem-208	254	11	nmr	nmr	NOUN
eurjchem-208	254	12	spectrum	spectrum	NOUN
eurjchem-208	254	13	at	at	ADP
eurjchem-208	254	14			NUM
eurjchem-208	254	15	18.4	18.4	NUM
eurjchem-208	254	16	ppm	ppm	NOUN
eurjchem-208	254	17	due	due	ADP
eurjchem-208	254	18	to	to	ADP
eurjchem-208	254	19	the	the	DET
eurjchem-208	254	20	presence	presence	NOUN
eurjchem-208	254	21	of	of	ADP
eurjchem-208	254	22	a	a	DET
eurjchem-208	254	23	hydro‐phosphoryl	hydro‐phosphoryl	NOUN
eurjchem-208	254	24	unit	unit	NOUN
eurjchem-208	254	25	[	[	X
eurjchem-208	254	26	28	28	NUM
eurjchem-208	254	27	]	]	PUNCT
eurjchem-208	254	28	.	.	PUNCT
eurjchem-208	255	1	the	the	DET
eurjchem-208	255	2	mass	mass	PROPN
eurjchem-208	255	3	spectral	spectral	ADJ
eurjchem-208	255	4	data	datum	NOUN
eurjchem-208	255	5	of	of	ADP
eurjchem-208	255	6	3a‐d	3a‐d	NOUN
eurjchem-208	255	7	were	be	AUX
eurjchem-208	255	8	in	in	ADP
eurjchem-208	255	9	accordance	accordance	NOUN
eurjchem-208	255	10	with	with	ADP
eurjchem-208	255	11	their	their	PRON
eurjchem-208	255	12	molecular	molecular	ADJ
eurjchem-208	255	13	formulas	formula	NOUN
eurjchem-208	255	14	.	.	PUNCT
eurjchem-208	256	1	scheme	scheme	VERB
eurjchem-208	256	2	2	2	NUM
eurjchem-208	256	3	a	a	DET
eurjchem-208	256	4	convenient	convenient	ADJ
eurjchem-208	256	5	procedure	procedure	NOUN
eurjchem-208	256	6	for	for	ADP
eurjchem-208	256	7	the	the	DET
eurjchem-208	256	8	synthesis	synthesis	NOUN
eurjchem-208	256	9	of	of	ADP
eurjchem-208	256	10	4‐formyl‐	4‐formyl‐	NUM
eurjchem-208	256	11	pyrazole	pyrazole	NOUN
eurjchem-208	256	12	derivatives	derivative	NOUN
eurjchem-208	256	13	is	be	AUX
eurjchem-208	256	14	based	base	VERB
eurjchem-208	256	15	on	on	ADP
eurjchem-208	256	16	the	the	DET
eurjchem-208	256	17	vilsmeier‐haack	vilsmeier‐haack	NOUN
eurjchem-208	256	18	reactions	reaction	NOUN
eurjchem-208	256	19	with	with	ADP
eurjchem-208	256	20	methyl	methyl	NOUN
eurjchem-208	256	21	ketone	ketone	NOUN
eurjchem-208	256	22	aryl	aryl	NOUN
eurjchem-208	256	23	hydrazones	hydrazone	NOUN
eurjchem-208	256	24	[	[	X
eurjchem-208	256	25	29‐32	29‐32	NUM
eurjchem-208	256	26	]	]	PUNCT
eurjchem-208	256	27	.	.	PUNCT
eurjchem-208	257	1	thus	thus	ADV
eurjchem-208	257	2	,	,	PUNCT
eurjchem-208	257	3	application	application	NOUN
eurjchem-208	257	4	of	of	ADP
eurjchem-208	257	5	vilsmeier‐haack	vilsmeier‐haack	NOUN
eurjchem-208	257	6	reaction	reaction	NOUN
eurjchem-208	257	7	on	on	ADP
eurjchem-208	257	8	phosphonic‐	phosphonic‐	PROPN
eurjchem-208	257	9	dihydrazones	dihydrazones	PROPN
eurjchem-208	257	10	3a	3a	NUM
eurjchem-208	257	11	,	,	PUNCT
eurjchem-208	257	12	b	b	PRON
eurjchem-208	257	13	afforded	afford	VERB
eurjchem-208	257	14	bis{4‐formyl‐3‐aryl‐1h‐pyrazol‐1‐yl}phosphine	bis{4‐formyl‐3‐aryl‐1h‐pyrazol‐1‐yl}phosphine	NOUN
eurjchem-208	257	15	oxides	oxide	NOUN
eurjchem-208	257	16	(	(	PUNCT
eurjchem-208	257	17	4a	4a	NUM
eurjchem-208	257	18	,	,	PUNCT
eurjchem-208	257	19	b	b	NOUN
eurjchem-208	257	20	)	)	PUNCT
eurjchem-208	257	21	(	(	PUNCT
eurjchem-208	257	22	scheme	scheme	NOUN
eurjchem-208	257	23	3	3	NUM
eurjchem-208	257	24	)	)	PUNCT
eurjchem-208	257	25	.	.	PUNCT
eurjchem-208	258	1	the	the	DET
eurjchem-208	258	2	proposed	propose	VERB
eurjchem-208	258	3	mechanism	mechanism	NOUN
eurjchem-208	258	4	for	for	ADP
eurjchem-208	258	5	the	the	DET
eurjchem-208	258	6	formation	formation	NOUN
eurjchem-208	258	7	of	of	ADP
eurjchem-208	258	8	4a	4a	NUM
eurjchem-208	258	9	,	,	PUNCT
eurjchem-208	258	10	b	b	NUM
eurjchem-208	258	11	involved	involve	VERB
eurjchem-208	258	12	double	double	ADJ
eurjchem-208	258	13	formylation	formylation	NOUN
eurjchem-208	258	14	at	at	ADP
eurjchem-208	258	15	each	each	DET
eurjchem-208	258	16	methyl	methyl	NOUN
eurjchem-208	258	17	group	group	NOUN
eurjchem-208	258	18	of	of	ADP
eurjchem-208	258	19	phosphonicdihydrazones	phosphonicdihydrazone	NOUN
eurjchem-208	258	20	3a	3a	NUM
eurjchem-208	258	21	,	,	PUNCT
eurjchem-208	258	22	b	b	PROPN
eurjchem-208	258	23	,	,	PUNCT
eurjchem-208	258	24	followed	follow	VERB
eurjchem-208	258	25	by	by	ADP
eurjchem-208	258	26	self‐cyclization	self‐cyclization	NOUN
eurjchem-208	258	27	then	then	ADV
eurjchem-208	258	28	hydrolysis	hydrolysis	NOUN
eurjchem-208	258	29	in	in	ADP
eurjchem-208	258	30	basic	basic	ADJ
eurjchem-208	258	31	medium	medium	NOUN
eurjchem-208	258	32	(	(	PUNCT
eurjchem-208	258	33	scheme	scheme	NOUN
eurjchem-208	258	34	4	4	NUM
eurjchem-208	258	35	)	)	PUNCT
eurjchem-208	259	1	[	[	X
eurjchem-208	259	2	33	33	NUM
eurjchem-208	259	3	]	]	PUNCT
eurjchem-208	259	4	.	.	PUNCT
eurjchem-208	260	1	the	the	DET
eurjchem-208	260	2	ir	ir	PROPN
eurjchem-208	260	3	spectra	spectra	NOUN
eurjchem-208	260	4	of	of	ADP
eurjchem-208	260	5	compounds	compound	NOUN
eurjchem-208	260	6	4a	4a	NUM
eurjchem-208	260	7	,	,	PUNCT
eurjchem-208	260	8	b	b	NOUN
eurjchem-208	260	9	showed	show	VERB
eurjchem-208	260	10	two	two	NUM
eurjchem-208	260	11	strong	strong	ADJ
eurjchem-208	260	12	absorption	absorption	NOUN
eurjchem-208	260	13	bands	band	NOUN
eurjchem-208	260	14	at	at	ADP
eurjchem-208	260	15	1678‐	1678‐	NUM
eurjchem-208	260	16	1671	1671	NUM
eurjchem-208	260	17	and	and	CCONJ
eurjchem-208	260	18	1284‐1241	1284‐1241	NUM
eurjchem-208	260	19	cm‐1	cm‐1	NOUN
eurjchem-208	260	20	assignable	assignable	ADJ
eurjchem-208	260	21	to	to	ADP
eurjchem-208	260	22	cho	cho	NOUN
eurjchem-208	260	23	and	and	CCONJ
eurjchem-208	260	24	p	p	X
eurjchem-208	260	25	=	=	ADJ
eurjchem-208	260	26	o	o	ADJ
eurjchem-208	260	27	functional	functional	ADJ
eurjchem-208	260	28	groups	group	NOUN
eurjchem-208	260	29	,	,	PUNCT
eurjchem-208	260	30	respectively	respectively	ADV
eurjchem-208	260	31	.	.	PUNCT
eurjchem-208	261	1	the	the	DET
eurjchem-208	261	2	1h	1h	NUM
eurjchem-208	261	3	nmr	nmr	NOUN
eurjchem-208	261	4	spectra	spectra	NOUN
eurjchem-208	261	5	of	of	ADP
eurjchem-208	261	6	compounds	compound	NOUN
eurjchem-208	261	7	4a	4a	NUM
eurjchem-208	261	8	,	,	PUNCT
eurjchem-208	261	9	b	b	NUM
eurjchem-208	261	10	exhibited	exhibit	VERB
eurjchem-208	261	11	singlet	singlet	NOUN
eurjchem-208	261	12	signals	signal	NOUN
eurjchem-208	261	13	at	at	ADP
eurjchem-208	261	14			NUM
eurjchem-208	261	15	9.95−10.00	9.95−10.00	NUM
eurjchem-208	261	16	ppm	ppm	NOUN
eurjchem-208	261	17	for	for	ADP
eurjchem-208	261	18	the	the	DET
eurjchem-208	261	19	formyl	formyl	ADJ
eurjchem-208	261	20	protons	proton	NOUN
eurjchem-208	261	21	and	and	CCONJ
eurjchem-208	261	22	the	the	DET
eurjchem-208	261	23	protons	proton	NOUN
eurjchem-208	261	24	of	of	ADP
eurjchem-208	261	25	the	the	DET
eurjchem-208	261	26	pyrazole	pyrazole	NOUN
eurjchem-208	261	27	rings	ring	NOUN
eurjchem-208	261	28	in	in	ADP
eurjchem-208	261	29	position	position	NOUN
eurjchem-208	261	30	5	5	NUM
eurjchem-208	261	31	resonated	resonate	VERB
eurjchem-208	261	32	at	at	ADP
eurjchem-208	261	33			PROPN
eurjchem-208	261	34	8.69−8.84	8.69−8.84	PROPN
eurjchem-208	261	35	ppm	ppm	PROPN
eurjchem-208	261	36	.	.	PUNCT
eurjchem-208	262	1	in	in	ADP
eurjchem-208	262	2	addition	addition	NOUN
eurjchem-208	262	3	,	,	PUNCT
eurjchem-208	262	4	doublet	doublet	ADJ
eurjchem-208	262	5	signals	signal	NOUN
eurjchem-208	262	6	were	be	AUX
eurjchem-208	262	7	present	present	ADJ
eurjchem-208	262	8	at	at	ADP
eurjchem-208	262	9			PROPN
eurjchem-208	262	10	7.45−7.54	7.45−7.54	PROPN
eurjchem-208	262	11	ppm	ppm	NOUN
eurjchem-208	262	12	(	(	PUNCT
eurjchem-208	262	13	jph=	jph=	PROPN
eurjchem-208	262	14	682–733	682–733	NUM
eurjchem-208	262	15	hz	hz	NOUN
eurjchem-208	262	16	)	)	PUNCT
eurjchem-208	262	17	corresponding	correspond	VERB
eurjchem-208	262	18	to	to	ADP
eurjchem-208	262	19	proton	proton	NOUN
eurjchem-208	262	20	of	of	ADP
eurjchem-208	262	21	h−p	h−p	NOUN
eurjchem-208	262	22	=	=	ADJ
eurjchem-208	262	23	o	o	NOUN
eurjchem-208	262	24	units	unit	NOUN
eurjchem-208	262	25	.	.	PUNCT
eurjchem-208	263	1	furthermore	furthermore	ADV
eurjchem-208	263	2	,	,	PUNCT
eurjchem-208	263	3	the	the	DET
eurjchem-208	263	4	13c	13c	NOUN
eurjchem-208	263	5	nmr	nmr	NOUN
eurjchem-208	263	6	spectrum	spectrum	NOUN
eurjchem-208	263	7	of	of	ADP
eurjchem-208	263	8	4a	4a	NUM
eurjchem-208	263	9	displayed	display	VERB
eurjchem-208	263	10	two	two	NUM
eurjchem-208	263	11	characteristic	characteristic	ADJ
eurjchem-208	263	12	signals	signal	NOUN
eurjchem-208	263	13	at	at	ADP
eurjchem-208	263	14			NUM
eurjchem-208	263	15	184.6	184.6	NUM
eurjchem-208	263	16	and	and	CCONJ
eurjchem-208	263	17	144.5	144.5	NUM
eurjchem-208	263	18	ppm	ppm	NOUN
eurjchem-208	263	19	corresponding	correspond	VERB
eurjchem-208	263	20	to	to	ADP
eurjchem-208	263	21	aldehydic	aldehydic	ADJ
eurjchem-208	263	22	carbon	carbon	NOUN
eurjchem-208	263	23	atom	atom	NOUN
eurjchem-208	263	24	and	and	CCONJ
eurjchem-208	263	25	c−5	c−5	PROPN
eurjchem-208	263	26	of	of	ADP
eurjchem-208	263	27	the	the	DET
eurjchem-208	263	28	pyrazole	pyrazole	NOUN
eurjchem-208	263	29	rings	ring	NOUN
eurjchem-208	263	30	,	,	PUNCT
eurjchem-208	263	31	respectively	respectively	ADV
eurjchem-208	263	32	.	.	PUNCT
eurjchem-208	264	1	also	also	ADV
eurjchem-208	264	2	,	,	PUNCT
eurjchem-208	264	3	the	the	DET
eurjchem-208	264	4	31p	31p	NUM
eurjchem-208	264	5	nmr	nmr	NOUN
eurjchem-208	264	6	spectrum	spectrum	NOUN
eurjchem-208	264	7	of	of	ADP
eurjchem-208	264	8	4b	4b	PROPN
eurjchem-208	264	9	showed	show	VERB
eurjchem-208	264	10	a	a	DET
eurjchem-208	264	11	signal	signal	NOUN
eurjchem-208	264	12	at	at	ADP
eurjchem-208	264	13			NUM
eurjchem-208	264	14	7.71	7.71	NUM
eurjchem-208	264	15	ppm	ppm	NOUN
eurjchem-208	264	16	.	.	PUNCT
eurjchem-208	265	1	mass	mass	PROPN
eurjchem-208	265	2	spectra	spectra	NOUN
eurjchem-208	265	3	of	of	ADP
eurjchem-208	265	4	4a	4a	NUM
eurjchem-208	265	5	,	,	PUNCT
eurjchem-208	265	6	b	b	PROPN
eurjchem-208	265	7	revealed	reveal	VERB
eurjchem-208	265	8	the	the	DET
eurjchem-208	265	9	molecular	molecular	ADJ
eurjchem-208	265	10	ion	ion	NOUN
eurjchem-208	265	11	peaks	peak	NOUN
eurjchem-208	265	12	at	at	ADP
eurjchem-208	265	13	m	m	PROPN
eurjchem-208	265	14	/	/	SYM
eurjchem-208	265	15	e	e	NOUN
eurjchem-208	265	16	389	389	NUM
eurjchem-208	265	17	(	(	PUNCT
eurjchem-208	265	18	m−h	m−h	NOUN
eurjchem-208	265	19	)	)	PUNCT
eurjchem-208	265	20	and	and	CCONJ
eurjchem-208	265	21	390	390	NUM
eurjchem-208	265	22	(	(	PUNCT
eurjchem-208	265	23	m−c12h8	m−c12h8	PROPN
eurjchem-208	265	24	)	)	PUNCT
eurjchem-208	265	25	,	,	PUNCT
eurjchem-208	265	26	respectively	respectively	ADV
eurjchem-208	265	27	.	.	PUNCT
eurjchem-208	266	1	n	n	PRON
eurjchem-208	266	2	h	h	NOUN
eurjchem-208	267	1	n	n	CCONJ
eurjchem-208	267	2	p	p	NOUN
eurjchem-208	267	3	h	h	NOUN
eurjchem-208	267	4	n	n	CCONJ
eurjchem-208	267	5	o	o	NOUN
eurjchem-208	267	6	h	h	NOUN
eurjchem-208	267	7	n	n	PROPN
eurjchem-208	267	8	ar	ar	PROPN
eurjchem-208	267	9	ch3	ch3	PROPN
eurjchem-208	267	10	ar	ar	PROPN
eurjchem-208	267	11	ch3	ch3	PROPN
eurjchem-208	267	12	3a	3a	PROPN
eurjchem-208	267	13	,	,	PUNCT
eurjchem-208	267	14	b	b	NOUN
eurjchem-208	267	15	4a	4a	NUM
eurjchem-208	267	16	,	,	PUNCT
eurjchem-208	267	17	b	b	PROPN
eurjchem-208	267	18	i	i	PROPN
eurjchem-208	267	19	)	)	PUNCT
eurjchem-208	267	20	pocl3	pocl3	PROPN
eurjchem-208	267	21	-	-	PUNCT
eurjchem-208	267	22	dmf	dmf	PROPN
eurjchem-208	267	23	ii	ii	PROPN
eurjchem-208	267	24	)	)	PUNCT
eurjchem-208	267	25	hydrolysis	hydrolysis	NOUN
eurjchem-208	267	26	n	n	ADP
eurjchem-208	267	27	n	n	NOUN
eurjchem-208	267	28	p	p	NOUN
eurjchem-208	267	29	n	n	CCONJ
eurjchem-208	267	30	n	n	PRON
eurjchem-208	267	31	h	h	NOUN
eurjchem-208	267	32	o	o	PROPN
eurjchem-208	267	33	ar	ar	PROPN
eurjchem-208	267	34	ar	ar	PROPN
eurjchem-208	267	35	choohc	choohc	PROPN
eurjchem-208	267	36	scheme	scheme	VERB
eurjchem-208	267	37	3	3	NUM
eurjchem-208	267	38	n	n	NOUN
eurjchem-208	267	39	h	h	NOUN
eurjchem-208	268	1	n	n	CCONJ
eurjchem-208	268	2	p	p	NOUN
eurjchem-208	268	3	h	h	NOUN
eurjchem-208	268	4	n	n	CCONJ
eurjchem-208	268	5	o	o	NOUN
eurjchem-208	268	6	h	h	NOUN
eurjchem-208	268	7	n	n	PROPN
eurjchem-208	268	8	ar	ar	PROPN
eurjchem-208	268	9	ch3	ch3	PROPN
eurjchem-208	268	10	ar	ar	PROPN
eurjchem-208	268	11	ch3	ch3	PROPN
eurjchem-208	268	12	n	n	PROPN
eurjchem-208	268	13	ch3	ch3	PROPN
eurjchem-208	269	1	ch3h	ch3h	PROPN
eurjchem-208	269	2	cl	cl	NOUN
eurjchem-208	270	1	p	p	NOUN
eurjchem-208	270	2	n	n	CCONJ
eurjchem-208	270	3	n	n	PROPN
eurjchem-208	270	4	ar	ar	NOUN
eurjchem-208	270	5	h	h	PROPN
eurjchem-208	270	6	n	n	PROPN
eurjchem-208	270	7	ch3	ch3	PROPN
eurjchem-208	270	8	ch3	ch3	PROPN
eurjchem-208	270	9	h	h	PROPN
eurjchem-208	270	10	n	n	PROPN
eurjchem-208	270	11	n	n	PROPN
eurjchem-208	270	12	ar	ar	PROPN
eurjchem-208	270	13	hn	hn	PROPN
eurjchem-208	270	14	ch3	ch3	PROPN
eurjchem-208	270	15	ch3	ch3	PROPN
eurjchem-208	270	16	h	h	PROPN
eurjchem-208	270	17	on	on	ADP
eurjchem-208	270	18	ch3	ch3	PROPN
eurjchem-208	270	19	ch3	ch3	PROPN
eurjchem-208	270	20	h	h	PROPN
eurjchem-208	270	21	n	n	PROPN
eurjchem-208	270	22	ch3	ch3	PROPN
eurjchem-208	270	23	ch3	ch3	PROPN
eurjchem-208	270	24	+	+	CCONJ
eurjchem-208	270	25	+	+	CCONJ
eurjchem-208	270	26	hydrolysis	hydrolysis	NOUN
eurjchem-208	270	27	2(ch3)2nh	2(ch3)2nh	NUM
eurjchem-208	270	28	3a	3a	NUM
eurjchem-208	270	29	,	,	PUNCT
eurjchem-208	270	30	b	b	NOUN
eurjchem-208	270	31	4a	4a	NUM
eurjchem-208	270	32	,	,	PUNCT
eurjchem-208	270	33	b	b	PROPN
eurjchem-208	270	34	+	+	CCONJ
eurjchem-208	270	35	n	n	PROPN
eurjchem-208	270	36	ar	ar	NOUN
eurjchem-208	270	37	n	n	PROPN
eurjchem-208	270	38	h	h	PROPN
eurjchem-208	270	39	n	n	ADP
eurjchem-208	270	40	ar	ar	PROPN
eurjchem-208	270	41	n	n	PROPN
eurjchem-208	270	42	h	h	NOUN
eurjchem-208	271	1	p	p	NOUN
eurjchem-208	271	2	h	h	NOUN
eurjchem-208	271	3	o	o	NOUN
eurjchem-208	271	4	n	n	CCONJ
eurjchem-208	271	5	ch3ch3	ch3ch3	ADJ
eurjchem-208	271	6	n	n	X
eurjchem-208	271	7	ch3	ch3	PROPN
eurjchem-208	271	8	ch3	ch3	PROPN
eurjchem-208	271	9	n	n	PROPN
eurjchem-208	271	10	ch3	ch3	PROPN
eurjchem-208	271	11	ch3	ch3	PROPN
eurjchem-208	271	12	n	n	PROPN
eurjchem-208	271	13	ch3	ch3	PROPN
eurjchem-208	271	14	ch3	ch3	PROPN
eurjchem-208	271	15	n	n	PROPN
eurjchem-208	271	16	ar	ar	PROPN
eurjchem-208	271	17	n	n	PROPN
eurjchem-208	271	18	h	h	PROPN
eurjchem-208	271	19	n	n	ADP
eurjchem-208	271	20	ar	ar	PROPN
eurjchem-208	271	21	n	n	PROPN
eurjchem-208	271	22	h	h	NOUN
eurjchem-208	272	1	p	p	NOUN
eurjchem-208	272	2	h	h	NOUN
eurjchem-208	273	1	o	o	NOUN
eurjchem-208	273	2	n	n	X
eurjchem-208	273	3	ch3	ch3	PROPN
eurjchem-208	273	4	ch3	ch3	PROPN
eurjchem-208	273	5	n	n	PROPN
eurjchem-208	273	6	ch3	ch3	PROPN
eurjchem-208	273	7	ch3	ch3	PROPN
eurjchem-208	273	8	2	2	PROPN
eurjchem-208	273	9	n	n	PROPN
eurjchem-208	273	10	ch3	ch3	NOUN
eurjchem-208	273	11	ch3h	ch3h	DET
eurjchem-208	273	12	cl	cl	NOUN
eurjchem-208	274	1	+	+	CCONJ
eurjchem-208	274	2	2	2	NUM
eurjchem-208	274	3	aq	aq	NOUN
eurjchem-208	274	4	.	.	PUNCT
eurjchem-208	274	5	ch3coona	ch3coona	PUNCT
eurjchem-208	275	1	+	+	NOUN
eurjchem-208	276	1	+	+	ADJ
eurjchem-208	276	2	+	+	SYM
eurjchem-208	276	3	+	+	CCONJ
eurjchem-208	276	4	n	n	PRON
eurjchem-208	276	5	ch3	ch3	PROPN
eurjchem-208	276	6	ch3	ch3	PROPN
eurjchem-208	276	7	o	o	PROPN
eurjchem-208	276	8	h	h	PROPN
eurjchem-208	276	9	+	+	CCONJ
eurjchem-208	276	10	pocl3	pocl3	PROPN
eurjchem-208	276	11	n	n	PROPN
eurjchem-208	276	12	ch3	ch3	PROPN
eurjchem-208	276	13	ch3	ch3	PROPN
eurjchem-208	276	14	opocl2	opocl2	PROPN
eurjchem-208	277	1	h	h	PROPN
eurjchem-208	277	2	cl	cl	PROPN
eurjchem-208	277	3	n	n	PROPN
eurjchem-208	277	4	ch3	ch3	PROPN
eurjchem-208	277	5	ch3	ch3	PROPN
eurjchem-208	277	6	h	h	PROPN
eurjchem-208	277	7	cl	cl	PROPN
eurjchem-208	277	8	opocl2	opocl2	PROPN
eurjchem-208	277	9	+	+	CCONJ
eurjchem-208	277	10	(	(	PUNCT
eurjchem-208	277	11	vilsmeier	vilsmeier	ADJ
eurjchem-208	277	12	reagent	reagent	NOUN
eurjchem-208	277	13	)	)	PUNCT
eurjchem-208	277	14	opocl2	opocl2	NOUN
eurjchem-208	277	15	opocl2	opocl2	NOUN
eurjchem-208	278	1	+	+	CCONJ
eurjchem-208	278	2	+	+	CCONJ
eurjchem-208	278	3	p	p	NOUN
eurjchem-208	278	4	n	n	CCONJ
eurjchem-208	278	5	n	n	ADP
eurjchem-208	278	6	ar	ar	PROPN
eurjchem-208	278	7	n	n	CCONJ
eurjchem-208	278	8	n	n	PROPN
eurjchem-208	278	9	ar	ar	NOUN
eurjchem-208	278	10	h	h	PROPN
eurjchem-208	278	11	on	on	ADP
eurjchem-208	278	12	ch3	ch3	PROPN
eurjchem-208	278	13	ch3	ch3	PROPN
eurjchem-208	278	14	n	n	PROPN
eurjchem-208	278	15	ch3	ch3	PROPN
eurjchem-208	278	16	ch3	ch3	PROPN
eurjchem-208	278	17	+	+	PROPN
eurjchem-208	279	1	+	+	CCONJ
eurjchem-208	279	2	p	p	NOUN
eurjchem-208	279	3	n	n	CCONJ
eurjchem-208	279	4	n	n	ADP
eurjchem-208	279	5	ar	ar	PROPN
eurjchem-208	279	6	n	n	CCONJ
eurjchem-208	279	7	n	n	PROPN
eurjchem-208	279	8	ar	ar	NOUN
eurjchem-208	279	9	h	h	NOUN
eurjchem-208	279	10	o	o	NOUN
eurjchem-208	279	11	choohc	choohc	NOUN
eurjchem-208	279	12	scheme	scheme	VERB
eurjchem-208	279	13	4	4	NUM
eurjchem-208	279	14	bis(4‐formylpyrazolyl)phosphine	bis(4‐formylpyrazolyl)phosphine	PROPN
eurjchem-208	279	15	oxides	oxide	NOUN
eurjchem-208	279	16	4a	4a	NUM
eurjchem-208	279	17	,	,	PUNCT
eurjchem-208	279	18	b	b	PROPN
eurjchem-208	279	19	were	be	AUX
eurjchem-208	279	20	oxidized	oxidize	VERB
eurjchem-208	279	21	in	in	ADP
eurjchem-208	279	22	basic	basic	ADJ
eurjchem-208	279	23	medium	medium	NOUN
eurjchem-208	279	24	by	by	ADP
eurjchem-208	279	25	potassium	potassium	NOUN
eurjchem-208	279	26	permanganate	permanganate	NOUN
eurjchem-208	279	27	to	to	PART
eurjchem-208	279	28	give	give	VERB
eurjchem-208	279	29	the	the	DET
eurjchem-208	279	30	corresponding	corresponding	ADJ
eurjchem-208	279	31	bis(4‐carboxypyrazolyl)phosphine	bis(4‐carboxypyrazolyl)phosphine	ADJ
eurjchem-208	279	32	oxides	oxide	NOUN
eurjchem-208	279	33	5a	5a	NUM
eurjchem-208	279	34	,	,	PUNCT
eurjchem-208	279	35	b	b	NOUN
eurjchem-208	279	36	,	,	PUNCT
eurjchem-208	279	37	respectively	respectively	ADV
eurjchem-208	279	38	(	(	PUNCT
eurjchem-208	279	39	scheme	scheme	NOUN
eurjchem-208	279	40	5	5	NUM
eurjchem-208	279	41	)	)	PUNCT
eurjchem-208	279	42	.	.	PUNCT
eurjchem-208	280	1	the	the	DET
eurjchem-208	280	2	oxidation	oxidation	NOUN
eurjchem-208	280	3	reaction	reaction	NOUN
eurjchem-208	280	4	took	take	VERB
eurjchem-208	280	5	place	place	NOUN
eurjchem-208	280	6	only	only	ADV
eurjchem-208	280	7	on	on	ADP
eurjchem-208	280	8	the	the	DET
eurjchem-208	280	9	formyl	formyl	ADJ
eurjchem-208	280	10	groups	group	NOUN
eurjchem-208	280	11	.	.	PUNCT
eurjchem-208	281	1	this	this	PRON
eurjchem-208	281	2	may	may	AUX
eurjchem-208	281	3	be	be	AUX
eurjchem-208	281	4	due	due	ADJ
eurjchem-208	281	5	to	to	ADP
eurjchem-208	281	6	the	the	DET
eurjchem-208	281	7	phosphorus	phosphorus	NOUN
eurjchem-208	281	8	centres	centre	NOUN
eurjchem-208	281	9	in	in	ADP
eurjchem-208	281	10	4a	4a	NUM
eurjchem-208	281	11	,	,	PUNCT
eurjchem-208	281	12	b	b	NOUN
eurjchem-208	281	13	are	be	AUX
eurjchem-208	281	14	less	less	ADV
eurjchem-208	281	15	susceptible	susceptible	ADJ
eurjchem-208	281	16	to	to	ADP
eurjchem-208	281	17	electrophiles	electrophile	NOUN
eurjchem-208	281	18	,	,	PUNCT
eurjchem-208	281	19	and	and	CCONJ
eurjchem-208	281	20	ultimately	ultimately	ADV
eurjchem-208	281	21	more	more	ADV
eurjchem-208	281	22	stable	stable	ADJ
eurjchem-208	281	23	and	and	CCONJ
eurjchem-208	281	24	resistant	resistant	ADJ
eurjchem-208	281	25	to	to	ADP
eurjchem-208	281	26	spontaneous	spontaneous	ADJ
eurjchem-208	281	27	oxidation	oxidation	NOUN
eurjchem-208	281	28	.	.	PUNCT
eurjchem-208	282	1	structures	structure	NOUN
eurjchem-208	282	2	of	of	ADP
eurjchem-208	282	3	products	product	NOUN
eurjchem-208	282	4	5a	5a	NUM
eurjchem-208	282	5	,	,	PUNCT
eurjchem-208	282	6	b	b	PROPN
eurjchem-208	282	7	were	be	AUX
eurjchem-208	282	8	established	establish	VERB
eurjchem-208	282	9	on	on	ADP
eurjchem-208	282	10	the	the	DET
eurjchem-208	282	11	basis	basis	NOUN
eurjchem-208	282	12	of	of	ADP
eurjchem-208	282	13	their	their	PRON
eurjchem-208	282	14	elemental	elemental	ADJ
eurjchem-208	282	15	and	and	CCONJ
eurjchem-208	282	16	spectral	spectral	ADJ
eurjchem-208	282	17	data	datum	NOUN
eurjchem-208	282	18	(	(	PUNCT
eurjchem-208	282	19	see	see	VERB
eurjchem-208	282	20	experimental	experimental	ADJ
eurjchem-208	282	21	section	section	NOUN
eurjchem-208	282	22	)	)	PUNCT
eurjchem-208	282	23	.	.	PUNCT
eurjchem-208	283	1	the	the	DET
eurjchem-208	283	2	present	present	ADJ
eurjchem-208	283	3	work	work	NOUN
eurjchem-208	283	4	was	be	AUX
eurjchem-208	283	5	also	also	ADV
eurjchem-208	283	6	extended	extend	VERB
eurjchem-208	283	7	to	to	PART
eurjchem-208	283	8	apply	apply	VERB
eurjchem-208	283	9	the	the	DET
eurjchem-208	283	10	vilsmeier‐haack	vilsmeier‐haack	NOUN
eurjchem-208	283	11	reaction	reaction	NOUN
eurjchem-208	283	12	on	on	ADP
eurjchem-208	283	13	phosphonicdihydrazones	phosphonicdihydrazone	NOUN
eurjchem-208	283	14	3c	3c	NUM
eurjchem-208	283	15	,	,	PUNCT
eurjchem-208	283	16	d	d	PROPN
eurjchem-208	283	17	which	which	PRON
eurjchem-208	283	18	contain	contain	VERB
eurjchem-208	283	19	active	active	ADJ
eurjchem-208	283	20	functional	functional	ADJ
eurjchem-208	283	21	groups	group	NOUN
eurjchem-208	283	22	in	in	ADP
eurjchem-208	283	23	ortho	ortho	PROPN
eurjchem-208	283	24	positions	position	NOUN
eurjchem-208	283	25	that	that	PRON
eurjchem-208	283	26	led	lead	VERB
eurjchem-208	283	27	to	to	ADP
eurjchem-208	283	28	new	new	ADJ
eurjchem-208	283	29	fused	fuse	VERB
eurjchem-208	283	30	pyrazole	pyrazole	NOUN
eurjchem-208	283	31	systems	system	NOUN
eurjchem-208	283	32	.	.	PUNCT
eurjchem-208	284	1	thus	thus	ADV
eurjchem-208	284	2	,	,	PUNCT
eurjchem-208	284	3	when	when	SCONJ
eurjchem-208	284	4	phosphonicdihydrazone	phosphonicdihydrazone	NOUN
eurjchem-208	284	5	3c	3c	NUM
eurjchem-208	284	6	was	be	AUX
eurjchem-208	284	7	treated	treat	VERB
eurjchem-208	284	8	with	with	ADP
eurjchem-208	284	9	vilsmeier	vilsmeier	ADJ
eurjchem-208	284	10	reagent	reagent	NOUN
eurjchem-208	284	11	afforded	afford	VERB
eurjchem-208	284	12	a	a	DET
eurjchem-208	284	13	red	red	ADJ
eurjchem-208	284	14	crystalline	crystalline	NOUN
eurjchem-208	284	15	product	product	NOUN
eurjchem-208	284	16	namely	namely	ADV
eurjchem-208	284	17	,	,	PUNCT
eurjchem-208	284	18	bis{2,4‐	bis{2,4‐	ADJ
eurjchem-208	284	19	dihydrochromeno[4,3‐c]pyrazol‐4‐hydroxy‐2‐yl}phosphine	dihydrochromeno[4,3‐c]pyrazol‐4‐hydroxy‐2‐yl}phosphine	PROPN
eurjchem-208	284	20	oxide	oxide	NOUN
eurjchem-208	284	21	(	(	PUNCT
eurjchem-208	284	22	6	6	NUM
eurjchem-208	284	23	)	)	PUNCT
eurjchem-208	284	24	.	.	PUNCT
eurjchem-208	285	1	formation	formation	NOUN
eurjchem-208	285	2	of	of	ADP
eurjchem-208	285	3	compound	compound	NOUN
eurjchem-208	285	4	6	6	NUM
eurjchem-208	285	5	involved	involve	VERB
eurjchem-208	285	6	double	double	ADJ
eurjchem-208	285	7	formylation	formylation	NOUN
eurjchem-208	285	8	at	at	ADP
eurjchem-208	285	9	the	the	DET
eurjchem-208	285	10	methyl	methyl	NOUN
eurjchem-208	285	11	groups	group	NOUN
eurjchem-208	285	12	of	of	ADP
eurjchem-208	285	13	3c	3c	NUM
eurjchem-208	285	14	,	,	PUNCT
eurjchem-208	285	15	followed	follow	VERB
eurjchem-208	285	16	by	by	ADP
eurjchem-208	285	17	30	30	NUM
eurjchem-208	285	18	abdel‐aziz	abdel‐aziz	NOUN
eurjchem-208	285	19	et	et	PROPN
eurjchem-208	285	20	al	al	PROPN
eurjchem-208	285	21	.	.	PUNCT
eurjchem-208	285	22	/	/	SYM
eurjchem-208	285	23	european	european	PROPN
eurjchem-208	285	24	journal	journal	PROPN
eurjchem-208	285	25	of	of	ADP
eurjchem-208	285	26	chemistry	chemistry	NOUN
eurjchem-208	285	27	2	2	NUM
eurjchem-208	285	28	(	(	PUNCT
eurjchem-208	285	29	1	1	NUM
eurjchem-208	285	30	)	)	PUNCT
eurjchem-208	285	31	(	(	PUNCT
eurjchem-208	285	32	2011	2011	NUM
eurjchem-208	285	33	)	)	PUNCT
eurjchem-208	285	34	25‐35	25‐35	NUM
eurjchem-208	285	35	nucleophilic	nucleophilic	ADJ
eurjchem-208	285	36	attack	attack	NOUN
eurjchem-208	285	37	of	of	ADP
eurjchem-208	285	38	nh	nh	PROPN
eurjchem-208	285	39	groups	group	NOUN
eurjchem-208	285	40	at	at	ADP
eurjchem-208	285	41	–	–	PUNCT
eurjchem-208	285	42	ch	ch	NOUN
eurjchem-208	285	43	=	=	NOUN
eurjchem-208	285	44	n+(ch3)2	n+(ch3)2	ADJ
eurjchem-208	285	45	moieties	moiety	NOUN
eurjchem-208	285	46	to	to	PART
eurjchem-208	285	47	eliminate	eliminate	VERB
eurjchem-208	285	48	two	two	NUM
eurjchem-208	285	49	molecules	molecule	NOUN
eurjchem-208	285	50	of	of	ADP
eurjchem-208	285	51	dimethylamine	dimethylamine	NOUN
eurjchem-208	285	52	.	.	PUNCT
eurjchem-208	286	1	another	another	DET
eurjchem-208	286	2	nucleo‐	nucleo‐	PROPN
eurjchem-208	286	3	philic	philic	ADJ
eurjchem-208	286	4	attack	attack	NOUN
eurjchem-208	286	5	took	take	VERB
eurjchem-208	286	6	place	place	NOUN
eurjchem-208	286	7	by	by	ADP
eurjchem-208	286	8	phenolic	phenolic	ADJ
eurjchem-208	286	9	oh	oh	NUM
eurjchem-208	286	10	groups	group	NOUN
eurjchem-208	286	11	at	at	ADP
eurjchem-208	286	12	–	–	PUNCT
eurjchem-208	286	13	ch	ch	NOUN
eurjchem-208	286	14	=	=	NOUN
eurjchem-208	286	15	n+(ch3)2	n+(ch3)2	ADJ
eurjchem-208	286	16	moieties	moiety	NOUN
eurjchem-208	286	17	,	,	PUNCT
eurjchem-208	286	18	followed	follow	VERB
eurjchem-208	286	19	by	by	ADP
eurjchem-208	286	20	hydrolysis	hydrolysis	NOUN
eurjchem-208	286	21	to	to	PART
eurjchem-208	286	22	give	give	VERB
eurjchem-208	286	23	the	the	DET
eurjchem-208	286	24	final	final	ADJ
eurjchem-208	286	25	product	product	NOUN
eurjchem-208	286	26	(	(	PUNCT
eurjchem-208	286	27	scheme	scheme	NOUN
eurjchem-208	286	28	6	6	NUM
eurjchem-208	286	29	)	)	PUNCT
eurjchem-208	286	30	.	.	PUNCT
eurjchem-208	287	1	the	the	DET
eurjchem-208	287	2	spectral	spectral	ADJ
eurjchem-208	287	3	data	datum	NOUN
eurjchem-208	287	4	of	of	ADP
eurjchem-208	287	5	6	6	NUM
eurjchem-208	287	6	recommended	recommend	VERB
eurjchem-208	287	7	the	the	DET
eurjchem-208	287	8	cyclic	cyclic	ADJ
eurjchem-208	287	9	structure	structure	NOUN
eurjchem-208	287	10	as	as	SCONJ
eurjchem-208	287	11	its	its	PRON
eurjchem-208	287	12	1h	1h	NUM
eurjchem-208	287	13	nmr	nmr	NOUN
eurjchem-208	287	14	spectrum	spectrum	NOUN
eurjchem-208	287	15	displayed	display	VERB
eurjchem-208	287	16	a	a	DET
eurjchem-208	287	17	broad	broad	ADJ
eurjchem-208	287	18	singlet	singlet	NOUN
eurjchem-208	287	19	(	(	PUNCT
eurjchem-208	287	20	d2o	d2o	NOUN
eurjchem-208	287	21	exchangeable	exchangeable	ADJ
eurjchem-208	287	22	)	)	PUNCT
eurjchem-208	287	23	at	at	ADP
eurjchem-208	287	24			NUM
eurjchem-208	287	25	3.72	3.72	NUM
eurjchem-208	287	26	ppm	ppm	NOUN
eurjchem-208	287	27	due	due	ADP
eurjchem-208	287	28	to	to	ADP
eurjchem-208	287	29	alcoholic	alcoholic	ADJ
eurjchem-208	287	30	oh	oh	INTJ
eurjchem-208	287	31	protons	proton	NOUN
eurjchem-208	287	32	and	and	CCONJ
eurjchem-208	287	33	singlet	singlet	ADJ
eurjchem-208	287	34	signal	signal	NOUN
eurjchem-208	287	35	at	at	ADP
eurjchem-208	287	36			NUM
eurjchem-208	287	37	6.53	6.53	NUM
eurjchem-208	287	38	ppm	ppm	NOUN
eurjchem-208	287	39	indicated	indicate	VERB
eurjchem-208	287	40	to	to	PART
eurjchem-208	287	41	h–2	h–2	VERB
eurjchem-208	287	42	proton	proton	NOUN
eurjchem-208	287	43	of	of	ADP
eurjchem-208	287	44	hydrochromene	hydrochromene	NOUN
eurjchem-208	287	45	moieties	moiety	NOUN
eurjchem-208	287	46	.	.	PUNCT
eurjchem-208	288	1	the	the	DET
eurjchem-208	288	2	protons	proton	NOUN
eurjchem-208	288	3	of	of	ADP
eurjchem-208	288	4	the	the	DET
eurjchem-208	288	5	formed	form	VERB
eurjchem-208	288	6	pyrazole	pyrazole	NOUN
eurjchem-208	288	7	rings	ring	NOUN
eurjchem-208	288	8	were	be	AUX
eurjchem-208	288	9	also	also	ADV
eurjchem-208	288	10	observed	observe	VERB
eurjchem-208	288	11	in	in	ADP
eurjchem-208	288	12	1h	1h	NUM
eurjchem-208	288	13	nmr	nmr	NOUN
eurjchem-208	288	14	spectrum	spectrum	NOUN
eurjchem-208	288	15	at	at	ADP
eurjchem-208	288	16			NUM
eurjchem-208	288	17	7.96	7.96	NUM
eurjchem-208	288	18	ppm	ppm	NOUN
eurjchem-208	288	19	while	while	SCONJ
eurjchem-208	288	20	proton	proton	NOUN
eurjchem-208	288	21	of	of	ADP
eurjchem-208	288	22	hydrophosphoryl	hydrophosphoryl	ADJ
eurjchem-208	288	23	unit	unit	NOUN
eurjchem-208	288	24	at	at	ADP
eurjchem-208	288	25			NUM
eurjchem-208	288	26	7.44	7.44	NUM
eurjchem-208	288	27	ppm	ppm	NOUN
eurjchem-208	288	28	(	(	PUNCT
eurjchem-208	288	29	jph	jph	NOUN
eurjchem-208	288	30	=	=	SYM
eurjchem-208	288	31	423	423	NUM
eurjchem-208	288	32	hz	hz	NOUN
eurjchem-208	288	33	)	)	PUNCT
eurjchem-208	288	34	,	,	PUNCT
eurjchem-208	288	35	respectively	respectively	ADV
eurjchem-208	288	36	.	.	PUNCT
eurjchem-208	289	1	also	also	ADV
eurjchem-208	289	2	,	,	PUNCT
eurjchem-208	289	3	its	its	PRON
eurjchem-208	289	4	ir	ir	PROPN
eurjchem-208	289	5	spectrum	spectrum	NOUN
eurjchem-208	289	6	showed	show	VERB
eurjchem-208	289	7	a	a	DET
eurjchem-208	289	8	broad	broad	ADJ
eurjchem-208	289	9	band	band	NOUN
eurjchem-208	289	10	at	at	ADP
eurjchem-208	289	11	3135	3135	NUM
eurjchem-208	289	12	cm‐1	cm‐1	NOUN
eurjchem-208	289	13	due	due	ADP
eurjchem-208	289	14	to	to	ADP
eurjchem-208	289	15	alcoholic	alcoholic	ADJ
eurjchem-208	289	16	oh	oh	INTJ
eurjchem-208	289	17	group	group	NOUN
eurjchem-208	289	18	.	.	PUNCT
eurjchem-208	290	1	the	the	DET
eurjchem-208	290	2	oxidation	oxidation	NOUN
eurjchem-208	290	3	reaction	reaction	NOUN
eurjchem-208	290	4	of	of	ADP
eurjchem-208	290	5	compound	compound	NOUN
eurjchem-208	290	6	6	6	NUM
eurjchem-208	290	7	with	with	ADP
eurjchem-208	290	8	selenium	selenium	NOUN
eurjchem-208	290	9	dioxide	dioxide	NOUN
eurjchem-208	290	10	in	in	ADP
eurjchem-208	290	11	dry	dry	ADJ
eurjchem-208	290	12	dioxane	dioxane	NOUN
eurjchem-208	290	13	yielded	yield	VERB
eurjchem-208	290	14	bis{chromeno[4,3‐c]pyrazol‐4‐oxo‐2‐yl}phosphine	bis{chromeno[4,3‐c]pyrazol‐4‐oxo‐2‐yl}phosphine	PROPN
eurjchem-208	290	15	oxide	oxide	NOUN
eurjchem-208	290	16	(	(	PUNCT
eurjchem-208	290	17	7	7	NUM
eurjchem-208	290	18	)	)	PUNCT
eurjchem-208	290	19	(	(	PUNCT
eurjchem-208	290	20	scheme	scheme	NOUN
eurjchem-208	290	21	7	7	NUM
eurjchem-208	290	22	)	)	PUNCT
eurjchem-208	290	23	.	.	PUNCT
eurjchem-208	291	1	the	the	DET
eurjchem-208	291	2	absorption	absorption	NOUN
eurjchem-208	291	3	band	band	NOUN
eurjchem-208	291	4	of	of	ADP
eurjchem-208	291	5	carbonyl	carbonyl	NOUN
eurjchem-208	291	6	groupappeared	groupappeare	VERB
eurjchem-208	291	7	at	at	ADP
eurjchem-208	291	8	1652	1652	NUM
eurjchem-208	291	9	cm‐1	cm‐1	NOUN
eurjchem-208	292	1	[	[	X
eurjchem-208	292	2	34,35	34,35	X
eurjchem-208	292	3	]	]	PUNCT
eurjchem-208	292	4	in	in	ADP
eurjchem-208	292	5	the	the	DET
eurjchem-208	292	6	ir	ir	PROPN
eurjchem-208	292	7	spectrum	spectrum	NOUN
eurjchem-208	292	8	of	of	ADP
eurjchem-208	292	9	7	7	NUM
eurjchem-208	292	10	.	.	PUNCT
eurjchem-208	293	1	also	also	ADV
eurjchem-208	293	2	,	,	PUNCT
eurjchem-208	293	3	its	its	PRON
eurjchem-208	293	4	structure	structure	NOUN
eurjchem-208	293	5	was	be	AUX
eurjchem-208	293	6	confirmed	confirm	VERB
eurjchem-208	293	7	from	from	ADP
eurjchem-208	293	8	1h	1h	NUM
eurjchem-208	293	9	nmr	nmr	NOUN
eurjchem-208	293	10	spectrum	spectrum	NOUN
eurjchem-208	293	11	by	by	ADP
eurjchem-208	293	12	disappearance	disappearance	NOUN
eurjchem-208	293	13	of	of	ADP
eurjchem-208	293	14	oh	oh	INTJ
eurjchem-208	293	15	and	and	CCONJ
eurjchem-208	293	16	c2	c2	PROPN
eurjchem-208	293	17	–	–	PUNCT
eurjchem-208	293	18	h	h	NOUN
eurjchem-208	293	19	protons	proton	NOUN
eurjchem-208	293	20	of	of	ADP
eurjchem-208	293	21	compound	compound	NOUN
eurjchem-208	293	22	6	6	NUM
eurjchem-208	293	23	.	.	PUNCT
eurjchem-208	294	1	scheme	scheme	NOUN
eurjchem-208	294	2	5	5	NUM
eurjchem-208	294	3	scheme	scheme	NOUN
eurjchem-208	294	4	6	6	NUM
eurjchem-208	294	5	scheme	scheme	NOUN
eurjchem-208	294	6	7	7	NUM
eurjchem-208	294	7	consequently	consequently	ADV
eurjchem-208	294	8	,	,	PUNCT
eurjchem-208	294	9	the	the	DET
eurjchem-208	294	10	effect	effect	NOUN
eurjchem-208	294	11	of	of	ADP
eurjchem-208	294	12	vilsmeier	vilsmeier	ADJ
eurjchem-208	294	13	reagent	reagent	NOUN
eurjchem-208	294	14	on	on	ADP
eurjchem-208	294	15	the	the	DET
eurjchem-208	294	16	phosphonicdihydrazone	phosphonicdihydrazone	NOUN
eurjchem-208	294	17	3d	3d	PROPN
eurjchem-208	294	18	afforded	afford	VERB
eurjchem-208	294	19	bis{chromeno[2,3‐g	bis{chromeno[2,3‐g	PROPN
eurjchem-208	294	20	]	]	X
eurjchem-208	294	21	indazol‐11‐oxo‐2‐yl}phosphine	indazol‐11‐oxo‐2‐yl}phosphine	PROPN
eurjchem-208	294	22	oxide	oxide	NOUN
eurjchem-208	294	23	(	(	PUNCT
eurjchem-208	294	24	8)	8)	NUM
eurjchem-208	294	25	in	in	ADP
eurjchem-208	294	26	moderate	moderate	ADJ
eurjchem-208	294	27	yield	yield	NOUN
eurjchem-208	294	28	(	(	PUNCT
eurjchem-208	294	29	scheme	scheme	NOUN
eurjchem-208	294	30	8)	8)	NUM
eurjchem-208	294	31	.	.	PUNCT
eurjchem-208	295	1	this	this	DET
eurjchem-208	295	2	transformation	transformation	NOUN
eurjchem-208	295	3	involved	involve	VERB
eurjchem-208	295	4	monoformylation	monoformylation	NOUN
eurjchem-208	295	5	at	at	ADP
eurjchem-208	295	6	each	each	DET
eurjchem-208	295	7	methyl	methyl	NOUN
eurjchem-208	295	8	group	group	NOUN
eurjchem-208	295	9	of	of	ADP
eurjchem-208	295	10	3d	3d	NUM
eurjchem-208	295	11	,	,	PUNCT
eurjchem-208	295	12	followed	follow	VERB
eurjchem-208	295	13	by	by	ADP
eurjchem-208	295	14	two	two	NUM
eurjchem-208	295	15	steps	step	NOUN
eurjchem-208	295	16	of	of	ADP
eurjchem-208	295	17	cyclization	cyclization	NOUN
eurjchem-208	295	18	process	process	NOUN
eurjchem-208	295	19	.	.	PUNCT
eurjchem-208	296	1	the	the	DET
eurjchem-208	296	2	first	first	ADJ
eurjchem-208	296	3	step	step	NOUN
eurjchem-208	296	4	is	be	AUX
eurjchem-208	296	5	nucleophilic	nucleophilic	ADJ
eurjchem-208	296	6	attack	attack	NOUN
eurjchem-208	296	7	of	of	ADP
eurjchem-208	296	8	nh	nh	PROPN
eurjchem-208	296	9	groups	group	NOUN
eurjchem-208	296	10	at	at	ADP
eurjchem-208	296	11	–	–	PUNCT
eurjchem-208	296	12	ch	ch	NOUN
eurjchem-208	296	13	=	=	NOUN
eurjchem-208	296	14	n+(ch3)2	n+(ch3)2	NOUN
eurjchem-208	296	15	to	to	PART
eurjchem-208	296	16	eliminate	eliminate	VERB
eurjchem-208	296	17	two	two	NUM
eurjchem-208	296	18	molecules	molecule	NOUN
eurjchem-208	296	19	of	of	ADP
eurjchem-208	296	20	dimethylamine	dimethylamine	NOUN
eurjchem-208	296	21	.	.	PUNCT
eurjchem-208	297	1	the	the	DET
eurjchem-208	297	2	second	second	ADJ
eurjchem-208	297	3	step	step	NOUN
eurjchem-208	297	4	is	be	AUX
eurjchem-208	297	5	nucleophilic	nucleophilic	ADJ
eurjchem-208	297	6	attack	attack	NOUN
eurjchem-208	297	7	of	of	ADP
eurjchem-208	297	8	the	the	DET
eurjchem-208	297	9	c–4	c–4	NOUN
eurjchem-208	297	10	of	of	ADP
eurjchem-208	297	11	formed	form	VERB
eurjchem-208	297	12	pyrazole	pyrazole	NOUN
eurjchem-208	297	13	rings	ring	NOUN
eurjchem-208	297	14	at	at	ADP
eurjchem-208	297	15	–	–	PUNCT
eurjchem-208	297	16	ch	ch	NOUN
eurjchem-208	297	17	=	=	NOUN
eurjchem-208	297	18	n+(ch3)2	n+(ch3)2	NOUN
eurjchem-208	297	19	of	of	ADP
eurjchem-208	297	20	chromone	chromone	NOUN
eurjchem-208	297	21	moieties	moiety	NOUN
eurjchem-208	297	22	to	to	PART
eurjchem-208	297	23	cyclize	cyclize	VERB
eurjchem-208	297	24	into	into	ADP
eurjchem-208	297	25	benzoid	benzoid	PROPN
eurjchem-208	297	26	system	system	NOUN
eurjchem-208	297	27	(	(	PUNCT
eurjchem-208	297	28	scheme	scheme	NOUN
eurjchem-208	297	29	8)	8)	NUM
eurjchem-208	297	30	[	[	X
eurjchem-208	297	31	36	36	NUM
eurjchem-208	297	32	]	]	PUNCT
eurjchem-208	297	33	.	.	PUNCT
eurjchem-208	298	1	the	the	DET
eurjchem-208	298	2	ir	ir	PROPN
eurjchem-208	298	3	spectrum	spectrum	NOUN
eurjchem-208	298	4	of	of	ADP
eurjchem-208	298	5	product	product	NOUN
eurjchem-208	298	6	8	8	NUM
eurjchem-208	298	7	showed	show	VERB
eurjchem-208	298	8	three	three	NUM
eurjchem-208	298	9	characteristic	characteristic	ADJ
eurjchem-208	298	10	absorption	absorption	NOUN
eurjchem-208	298	11	bands	band	NOUN
eurjchem-208	298	12	at	at	ADP
eurjchem-208	298	13	1646	1646	NUM
eurjchem-208	298	14	,	,	PUNCT
eurjchem-208	298	15	1596	1596	NUM
eurjchem-208	298	16	and	and	CCONJ
eurjchem-208	298	17	1569	1569	NUM
eurjchem-208	298	18	cm‐1	cm‐1	NOUN
eurjchem-208	298	19	assignable	assignable	ADJ
eurjchem-208	298	20	to	to	ADP
eurjchem-208	298	21	c	c	NOUN
eurjchem-208	298	22	=	=	SYM
eurjchem-208	298	23	o	o	NOUN
eurjchem-208	298	24	,	,	PUNCT
eurjchem-208	298	25	c	c	PROPN
eurjchem-208	298	26	=	=	SYM
eurjchem-208	298	27	n	n	NOUN
eurjchem-208	298	28	and	and	CCONJ
eurjchem-208	298	29	c	c	X
eurjchem-208	298	30	=	=	NOUN
eurjchem-208	298	31	c	c	X
eurjchem-208	298	32	functional	functional	ADJ
eurjchem-208	298	33	groups	group	NOUN
eurjchem-208	298	34	,	,	PUNCT
eurjchem-208	298	35	respectively	respectively	ADV
eurjchem-208	298	36	.	.	PUNCT
eurjchem-208	299	1	moreover	moreover	ADV
eurjchem-208	299	2	,	,	PUNCT
eurjchem-208	299	3	its	its	PRON
eurjchem-208	299	4	1h	1h	NUM
eurjchem-208	299	5	nmr	nmr	NOUN
eurjchem-208	299	6	spectrum	spectrum	NOUN
eurjchem-208	299	7	revealed	reveal	VERB
eurjchem-208	299	8	a	a	DET
eurjchem-208	299	9	singlet	singlet	ADJ
eurjchem-208	299	10	signal	signal	NOUN
eurjchem-208	299	11	of	of	ADP
eurjchem-208	299	12	c5	c5	PROPN
eurjchem-208	299	13	–	–	PUNCT
eurjchem-208	299	14	h	h	NOUN
eurjchem-208	299	15	of	of	ADP
eurjchem-208	299	16	pyrazole	pyrazole	NOUN
eurjchem-208	299	17	rings	ring	NOUN
eurjchem-208	299	18	at	at	ADP
eurjchem-208	299	19			NUM
eurjchem-208	299	20	7.89	7.89	NUM
eurjchem-208	299	21	ppm	ppm	NOUN
eurjchem-208	299	22	while	while	SCONJ
eurjchem-208	299	23	the	the	DET
eurjchem-208	299	24	aromatic	aromatic	ADJ
eurjchem-208	299	25	protons	proton	NOUN
eurjchem-208	299	26	at	at	ADP
eurjchem-208	299	27			NUM
eurjchem-208	299	28	7.05–7.80	7.05–7.80	NUM
eurjchem-208	299	29	ppm	ppm	NOUN
eurjchem-208	299	30	as	as	ADP
eurjchem-208	299	31	multiplet	multiplet	NOUN
eurjchem-208	299	32	signals	signal	NOUN
eurjchem-208	299	33	.	.	PUNCT
eurjchem-208	300	1	the	the	DET
eurjchem-208	300	2	mass	mass	PROPN
eurjchem-208	300	3	spectrum	spectrum	NOUN
eurjchem-208	300	4	of	of	ADP
eurjchem-208	300	5	8	8	NUM
eurjchem-208	300	6	showed	show	VERB
eurjchem-208	300	7	a	a	DET
eurjchem-208	300	8	molecular	molecular	ADJ
eurjchem-208	300	9	ion	ion	NOUN
eurjchem-208	300	10	peak	peak	NOUN
eurjchem-208	300	11	at	at	ADP
eurjchem-208	300	12	m	m	PROPN
eurjchem-208	300	13	/	/	SYM
eurjchem-208	300	14	e	e	NOUN
eurjchem-208	300	15	518	518	NUM
eurjchem-208	300	16	with	with	ADP
eurjchem-208	300	17	a	a	DET
eurjchem-208	300	18	base	base	NOUN
eurjchem-208	300	19	peak	peak	NOUN
eurjchem-208	300	20	at	at	ADP
eurjchem-208	300	21	m	m	PROPN
eurjchem-208	300	22	/	/	SYM
eurjchem-208	300	23	e	e	X
eurjchem-208	300	24	384	384	NUM
eurjchem-208	300	25	.	.	PUNCT
eurjchem-208	300	26	scheme	scheme	VERB
eurjchem-208	300	27	8	8	NUM
eurjchem-208	300	28	sulfur	sulfur	NOUN
eurjchem-208	300	29	and	and	CCONJ
eurjchem-208	300	30	phosphorus	phosphorus	NOUN
eurjchem-208	300	31	containing	contain	VERB
eurjchem-208	300	32	heterocyclic	heterocyclic	ADJ
eurjchem-208	300	33	compounds	compound	NOUN
eurjchem-208	300	34	play	play	VERB
eurjchem-208	300	35	an	an	DET
eurjchem-208	300	36	important	important	ADJ
eurjchem-208	300	37	role	role	NOUN
eurjchem-208	300	38	in	in	ADP
eurjchem-208	300	39	organic	organic	ADJ
eurjchem-208	300	40	chemistry	chemistry	NOUN
eurjchem-208	300	41	and	and	CCONJ
eurjchem-208	300	42	attract	attract	VERB
eurjchem-208	300	43	strong	strong	ADJ
eurjchem-208	300	44	interest	interest	NOUN
eurjchem-208	300	45	due	due	ADP
eurjchem-208	300	46	to	to	ADP
eurjchem-208	300	47	diversity	diversity	NOUN
eurjchem-208	300	48	of	of	ADP
eurjchem-208	300	49	their	their	PRON
eurjchem-208	300	50	chemical	chemical	NOUN
eurjchem-208	300	51	transformations	transformation	NOUN
eurjchem-208	300	52	and	and	CCONJ
eurjchem-208	300	53	broad	broad	ADJ
eurjchem-208	300	54	spectrum	spectrum	NOUN
eurjchem-208	300	55	of	of	ADP
eurjchem-208	300	56	biological	biological	ADJ
eurjchem-208	300	57	activity	activity	NOUN
eurjchem-208	300	58	[	[	X
eurjchem-208	300	59	37,38	37,38	NOUN
eurjchem-208	300	60	]	]	PUNCT
eurjchem-208	300	61	.	.	PUNCT
eurjchem-208	301	1	in	in	ADP
eurjchem-208	301	2	this	this	DET
eurjchem-208	301	3	research	research	NOUN
eurjchem-208	301	4	,	,	PUNCT
eurjchem-208	301	5	bis(4‐formylpyrazolyl)phosphine	bis(4‐formylpyrazolyl)phosphine	PROPN
eurjchem-208	301	6	oxides	oxide	NOUN
eurjchem-208	301	7	4a	4a	NUM
eurjchem-208	301	8	,	,	PUNCT
eurjchem-208	301	9	b	b	PROPN
eurjchem-208	301	10	turned	turn	VERB
eurjchem-208	301	11	out	out	ADP
eurjchem-208	301	12	to	to	PART
eurjchem-208	301	13	be	be	AUX
eurjchem-208	301	14	fairly	fairly	ADV
eurjchem-208	301	15	reactive	reactive	ADJ
eurjchem-208	301	16	compounds	compound	NOUN
eurjchem-208	301	17	,	,	PUNCT
eurjchem-208	301	18	and	and	CCONJ
eurjchem-208	301	19	they	they	PRON
eurjchem-208	301	20	readily	readily	ADV
eurjchem-208	301	21	condensed	condense	VERB
eurjchem-208	301	22	with	with	ADP
eurjchem-208	301	23	nitrogen	nitrogen	NOUN
eurjchem-208	301	24	and	and	CCONJ
eurjchem-208	301	25	carbon	carbon	NOUN
eurjchem-208	301	26	nucleophiles	nucleophile	NOUN
eurjchem-208	301	27	to	to	PART
eurjchem-208	301	28	give	give	VERB
eurjchem-208	301	29	the	the	DET
eurjchem-208	301	30	corresponding	correspond	VERB
eurjchem-208	301	31	condensation	condensation	NOUN
eurjchem-208	301	32	products	product	NOUN
eurjchem-208	301	33	.	.	PUNCT
eurjchem-208	302	1	the	the	DET
eurjchem-208	302	2	reactivity	reactivity	NOUN
eurjchem-208	302	3	of	of	ADP
eurjchem-208	302	4	these	these	DET
eurjchem-208	302	5	condensation	condensation	NOUN
eurjchem-208	302	6	products	product	NOUN
eurjchem-208	302	7	towards	towards	ADP
eurjchem-208	302	8	sulfur	sulfur	NOUN
eurjchem-208	302	9	and	and	CCONJ
eurjchem-208	302	10	phosphorus	phosphorus	NOUN
eurjchem-208	302	11	reagents	reagent	NOUN
eurjchem-208	302	12	was	be	AUX
eurjchem-208	302	13	investigated	investigate	VERB
eurjchem-208	302	14	.	.	PUNCT
eurjchem-208	303	1	thus	thus	ADV
eurjchem-208	303	2	,	,	PUNCT
eurjchem-208	303	3	treatment	treatment	NOUN
eurjchem-208	303	4	of	of	ADP
eurjchem-208	303	5	compound	compound	NOUN
eurjchem-208	303	6	4a	4a	NOUN
eurjchem-208	303	7	with	with	ADP
eurjchem-208	303	8	aniline	aniline	NOUN
eurjchem-208	303	9	,	,	PUNCT
eurjchem-208	303	10	in	in	ADP
eurjchem-208	303	11	refluxing	refluxing	NOUN
eurjchem-208	303	12	ethanol	ethanol	NOUN
eurjchem-208	303	13	,	,	PUNCT
eurjchem-208	303	14	afforded	afford	VERB
eurjchem-208	303	15	yellow	yellow	ADJ
eurjchem-208	303	16	crystals	crystal	NOUN
eurjchem-208	303	17	of	of	ADP
eurjchem-208	303	18	bis{3‐phenyl‐4‐	bis{3‐phenyl‐4‐	PROPN
eurjchem-208	303	19	[	[	X
eurjchem-208	303	20	(	(	PUNCT
eurjchem-208	303	21	phenylimino)methyl]‐1h‐pyrazol‐1‐yl}phosphine	phenylimino)methyl]‐1h‐pyrazol‐1‐yl}phosphine	NOUN
eurjchem-208	303	22	oxide	oxide	NOUN
eurjchem-208	303	23	(	(	PUNCT
eurjchem-208	303	24	9	9	NUM
eurjchem-208	303	25	)	)	PUNCT
eurjchem-208	303	26	(	(	PUNCT
eurjchem-208	303	27	scheme	scheme	NOUN
eurjchem-208	303	28	9	9	NUM
eurjchem-208	303	29	)	)	PUNCT
eurjchem-208	303	30	.	.	PUNCT
eurjchem-208	304	1	the	the	DET
eurjchem-208	304	2	structure	structure	NOUN
eurjchem-208	304	3	of	of	ADP
eurjchem-208	304	4	bis‐schiff	bis‐schiff	PROPN
eurjchem-208	304	5	's	's	PART
eurjchem-208	304	6	base	base	NOUN
eurjchem-208	304	7	9	9	NUM
eurjchem-208	304	8	was	be	AUX
eurjchem-208	304	9	confirmed	confirm	VERB
eurjchem-208	304	10	by	by	ADP
eurjchem-208	304	11	both	both	CCONJ
eurjchem-208	304	12	spectral	spectral	ADJ
eurjchem-208	304	13	and	and	CCONJ
eurjchem-208	304	14	elemental	elemental	ADJ
eurjchem-208	304	15	analysis	analysis	NOUN
eurjchem-208	304	16	(	(	PUNCT
eurjchem-208	304	17	see	see	VERB
eurjchem-208	304	18	experimental	experimental	ADJ
eurjchem-208	304	19	section	section	NOUN
eurjchem-208	304	20	)	)	PUNCT
eurjchem-208	304	21	.	.	PUNCT
eurjchem-208	305	1	when	when	SCONJ
eurjchem-208	305	2	bis‐schiff	bis‐schiff	PROPN
eurjchem-208	305	3	's	's	PART
eurjchem-208	305	4	base	base	NOUN
eurjchem-208	305	5	9	9	NUM
eurjchem-208	305	6	was	be	AUX
eurjchem-208	305	7	treated	treat	VERB
eurjchem-208	305	8	with	with	ADP
eurjchem-208	305	9	thioglycolic	thioglycolic	ADJ
eurjchem-208	305	10	acid	acid	NOUN
eurjchem-208	305	11	,	,	PUNCT
eurjchem-208	305	12	in	in	ADP
eurjchem-208	305	13	refluxing	refluxing	NOUN
eurjchem-208	305	14	dry	dry	PROPN
eurjchem-208	305	15	dmf	dmf	PROPN
eurjchem-208	305	16	containing	contain	VERB
eurjchem-208	305	17	anhydrous	anhydrous	ADJ
eurjchem-208	305	18	zinc	zinc	NOUN
eurjchem-208	305	19	chloride	chloride	NOUN
eurjchem-208	305	20	as	as	ADP
eurjchem-208	305	21	a	a	DET
eurjchem-208	305	22	catalyst	catalyst	NOUN
eurjchem-208	305	23	,	,	PUNCT
eurjchem-208	305	24	afforded	afford	VERB
eurjchem-208	305	25	a	a	DET
eurjchem-208	305	26	single	single	ADJ
eurjchem-208	305	27	product	product	NOUN
eurjchem-208	305	28	identified	identify	VERB
eurjchem-208	305	29	as	as	ADP
eurjchem-208	305	30	bis{3‐phenyl‐4‐	bis{3‐phenyl‐4‐	PROPN
eurjchem-208	305	31	[	[	X
eurjchem-208	305	32	3‐phenyl‐4‐oxo‐1,3‐thiazolidin‐2‐yl]‐1h‐pyrazol‐1‐yl}phos‐	3‐phenyl‐4‐oxo‐1,3‐thiazolidin‐2‐yl]‐1h‐pyrazol‐1‐yl}phos‐	NUM
eurjchem-208	305	33	phine	phine	NOUN
eurjchem-208	305	34	oxide	oxide	NOUN
eurjchem-208	305	35	(	(	PUNCT
eurjchem-208	305	36	10	10	NUM
eurjchem-208	305	37	)	)	PUNCT
eurjchem-208	305	38	.	.	PUNCT
eurjchem-208	306	1	the	the	DET
eurjchem-208	306	2	latter	latter	ADJ
eurjchem-208	306	3	compound	compound	NOUN
eurjchem-208	306	4	was	be	AUX
eurjchem-208	306	5	also	also	ADV
eurjchem-208	306	6	obtained	obtain	VERB
eurjchem-208	306	7	authentically	authentically	ADV
eurjchem-208	306	8	in	in	ADP
eurjchem-208	306	9	one‐pot	one‐pot	PROPN
eurjchem-208	306	10	(	(	PUNCT
eurjchem-208	306	11	four	four	NUM
eurjchem-208	306	12	components	component	NOUN
eurjchem-208	306	13	)	)	PUNCT
eurjchem-208	306	14	from	from	ADP
eurjchem-208	306	15	the	the	DET
eurjchem-208	306	16	direct	direct	ADJ
eurjchem-208	306	17	reaction	reaction	NOUN
eurjchem-208	306	18	of	of	ADP
eurjchem-208	306	19	4a	4a	NOUN
eurjchem-208	306	20	with	with	ADP
eurjchem-208	306	21	aniline	aniline	NOUN
eurjchem-208	306	22	and	and	CCONJ
eurjchem-208	306	23	thioglycolic	thioglycolic	ADJ
eurjchem-208	306	24	acid	acid	NOUN
eurjchem-208	306	25	in	in	ADP
eurjchem-208	306	26	the	the	DET
eurjchem-208	306	27	presence	presence	NOUN
eurjchem-208	306	28	of	of	ADP
eurjchem-208	306	29	anhydrous	anhydrous	ADJ
eurjchem-208	306	30	zinc	zinc	NOUN
eurjchem-208	306	31	chloride	chloride	NOUN
eurjchem-208	306	32	(	(	PUNCT
eurjchem-208	306	33	scheme	scheme	NOUN
eurjchem-208	306	34	9	9	NUM
eurjchem-208	306	35	)	)	PUNCT
eurjchem-208	306	36	.	.	PUNCT
eurjchem-208	307	1	the	the	DET
eurjchem-208	307	2	ir	ir	PROPN
eurjchem-208	307	3	spectrum	spectrum	NOUN
eurjchem-208	307	4	of	of	ADP
eurjchem-208	307	5	10	10	NUM
eurjchem-208	307	6	showed	show	VERB
eurjchem-208	307	7	the	the	DET
eurjchem-208	307	8	carbonyl	carbonyl	NOUN
eurjchem-208	307	9	groups	group	NOUN
eurjchem-208	307	10	of	of	ADP
eurjchem-208	307	11	thiazolidinone	thiazolidinone	NOUN
eurjchem-208	307	12	moieties	moiety	NOUN
eurjchem-208	307	13	at	at	ADP
eurjchem-208	307	14	1658	1658	NUM
eurjchem-208	307	15	cm‐1	cm‐1	NOUN
eurjchem-208	307	16	.	.	PUNCT
eurjchem-208	308	1	also	also	ADV
eurjchem-208	308	2	,	,	PUNCT
eurjchem-208	308	3	its	its	PRON
eurjchem-208	308	4	1h	1h	NUM
eurjchem-208	308	5	nmr	nmr	NOUN
eurjchem-208	308	6	spectrum	spectrum	NOUN
eurjchem-208	308	7	exhibited	exhibit	VERB
eurjchem-208	308	8	two	two	NUM
eurjchem-208	308	9	singlet	singlet	ADJ
eurjchem-208	308	10	signals	signal	NOUN
eurjchem-208	308	11	at	at	ADP
eurjchem-208	308	12			NUM
eurjchem-208	308	13	5.91	5.91	NUM
eurjchem-208	308	14	and	and	CCONJ
eurjchem-208	308	15	4.46	4.46	NUM
eurjchem-208	308	16	ppm	ppm	NOUN
eurjchem-208	308	17	due	due	ADP
eurjchem-208	308	18	to	to	ADP
eurjchem-208	308	19	c2	c2	PROPN
eurjchem-208	308	20	–	–	PUNCT
eurjchem-208	308	21	h	h	PROPN
eurjchem-208	308	22	and	and	CCONJ
eurjchem-208	308	23	ch2	ch2	PROPN
eurjchem-208	308	24	of	of	ADP
eurjchem-208	308	25	thiazolidinone	thiazolidinone	NOUN
eurjchem-208	308	26	protons	proton	NOUN
eurjchem-208	308	27	,	,	PUNCT
eurjchem-208	308	28	respectively	respectively	ADV
eurjchem-208	308	29	,	,	PUNCT
eurjchem-208	308	30	while	while	SCONJ
eurjchem-208	308	31	the	the	DET
eurjchem-208	308	32	proton	proton	NOUN
eurjchem-208	308	33	of	of	ADP
eurjchem-208	308	34	h	h	NOUN
eurjchem-208	308	35	–	–	PUNCT
eurjchem-208	308	36	p	p	X
eurjchem-208	308	37	=	=	NOUN
eurjchem-208	308	38	o	o	NOUN
eurjchem-208	308	39	appeared	appear	VERB
eurjchem-208	308	40	as	as	ADP
eurjchem-208	308	41	a	a	DET
eurjchem-208	308	42	doublet	doublet	ADJ
eurjchem-208	308	43	signal	signal	NOUN
eurjchem-208	308	44	at	at	ADP
eurjchem-208	308	45			NUM
eurjchem-208	308	46	7.28	7.28	NUM
eurjchem-208	308	47	ppm	ppm	NOUN
eurjchem-208	308	48	(	(	PUNCT
eurjchem-208	308	49	jph=	jph=	NOUN
eurjchem-208	308	50	454	454	NUM
eurjchem-208	308	51	hz	hz	NOUN
eurjchem-208	308	52	)	)	PUNCT
eurjchem-208	308	53	.	.	PUNCT
eurjchem-208	309	1	abdel‐aziz	abdel‐aziz	INTJ
eurjchem-208	310	1	et	et	PROPN
eurjchem-208	310	2	al./	al./	ADV
eurjchem-208	310	3	european	european	PROPN
eurjchem-208	310	4	journal	journal	PROPN
eurjchem-208	310	5	of	of	ADP
eurjchem-208	310	6	chemistry	chemistry	NOUN
eurjchem-208	310	7	2	2	NUM
eurjchem-208	310	8	(	(	PUNCT
eurjchem-208	310	9	1	1	NUM
eurjchem-208	310	10	)	)	PUNCT
eurjchem-208	310	11	(	(	PUNCT
eurjchem-208	310	12	2011	2011	NUM
eurjchem-208	310	13	)	)	PUNCT
eurjchem-208	310	14	25‐35	25‐35	NUM
eurjchem-208	310	15	31	31	NUM
eurjchem-208	310	16	scheme	scheme	NOUN
eurjchem-208	310	17	9	9	NUM
eurjchem-208	310	18	also	also	ADV
eurjchem-208	310	19	,	,	PUNCT
eurjchem-208	310	20	when	when	SCONJ
eurjchem-208	310	21	bis‐schiff	bis‐schiff	PROPN
eurjchem-208	310	22	's	's	PART
eurjchem-208	310	23	base	base	NOUN
eurjchem-208	310	24	9	9	NUM
eurjchem-208	310	25	was	be	AUX
eurjchem-208	310	26	treated	treat	VERB
eurjchem-208	310	27	with	with	ADP
eurjchem-208	310	28	diethyl	diethyl	NOUN
eurjchem-208	310	29	phosphite	phosphite	NOUN
eurjchem-208	310	30	in	in	ADP
eurjchem-208	310	31	the	the	DET
eurjchem-208	310	32	presence	presence	NOUN
eurjchem-208	310	33	of	of	ADP
eurjchem-208	310	34	bf3.et2o	bf3.et2o	PROPN
eurjchem-208	310	35	as	as	ADP
eurjchem-208	310	36	a	a	DET
eurjchem-208	310	37	catalyst	catalyst	NOUN
eurjchem-208	310	38	at	at	ADP
eurjchem-208	310	39	80	80	NUM
eurjchem-208	310	40	oc	oc	NOUN
eurjchem-208	310	41	under	under	ADP
eurjchem-208	310	42	pudovik	pudovik	NOUN
eurjchem-208	310	43	reaction	reaction	NOUN
eurjchem-208	310	44	condition	condition	NOUN
eurjchem-208	310	45	[	[	X
eurjchem-208	310	46	39	39	NUM
eurjchem-208	310	47	]	]	PUNCT
eurjchem-208	310	48	,	,	PUNCT
eurjchem-208	310	49	produced	produce	VERB
eurjchem-208	310	50	a	a	DET
eurjchem-208	310	51	novel	novel	ADJ
eurjchem-208	310	52	type	type	NOUN
eurjchem-208	310	53	of	of	ADP
eurjchem-208	310	54	bis(‐aminophosphonate	bis(‐aminophosphonate	NOUN
eurjchem-208	310	55	)	)	PUNCT
eurjchem-208	310	56	structure	structure	NOUN
eurjchem-208	310	57	11	11	NUM
eurjchem-208	310	58	,	,	PUNCT
eurjchem-208	310	59	which	which	PRON
eurjchem-208	310	60	was	be	AUX
eurjchem-208	310	61	also	also	ADV
eurjchem-208	310	62	obtainedauthenticallyin	obtainedauthenticallyin	X
eurjchem-208	310	63	high	high	ADJ
eurjchem-208	310	64	yield	yield	NOUN
eurjchem-208	310	65	in	in	ADP
eurjchem-208	310	66	one‐pot	one‐pot	PROPN
eurjchem-208	310	67	(	(	PUNCT
eurjchem-208	310	68	four	four	NUM
eurjchem-208	310	69	compo‐	compo‐	NOUN
eurjchem-208	310	70	nents	nent	NOUN
eurjchem-208	310	71	)	)	PUNCT
eurjchem-208	310	72	from	from	ADP
eurjchem-208	310	73	the	the	DET
eurjchem-208	310	74	direct	direct	ADJ
eurjchem-208	310	75	reaction	reaction	NOUN
eurjchem-208	310	76	of	of	ADP
eurjchem-208	310	77	4a	4a	NOUN
eurjchem-208	310	78	with	with	ADP
eurjchem-208	310	79	aniline	aniline	NOUN
eurjchem-208	310	80	and	and	CCONJ
eurjchem-208	310	81	diethyl	diethyl	NOUN
eurjchem-208	310	82	phosphite	phosphite	NOUN
eurjchem-208	310	83	in	in	ADP
eurjchem-208	310	84	the	the	DET
eurjchem-208	310	85	presence	presence	NOUN
eurjchem-208	310	86	of	of	ADP
eurjchem-208	310	87	bf3.et2o	bf3.et2o	PROPN
eurjchem-208	310	88	at	at	ADP
eurjchem-208	310	89	80	80	NUM
eurjchem-208	310	90	oc	oc	NOUN
eurjchem-208	310	91	under	under	ADP
eurjchem-208	310	92	kabachnik‐fields	kabachnik‐field	NOUN
eurjchem-208	310	93	reaction	reaction	NOUN
eurjchem-208	310	94	conditions	condition	NOUN
eurjchem-208	310	95	[	[	X
eurjchem-208	310	96	40	40	NUM
eurjchem-208	310	97	]	]	PUNCT
eurjchem-208	310	98	(	(	PUNCT
eurjchem-208	310	99	scheme	scheme	NOUN
eurjchem-208	310	100	9	9	NUM
eurjchem-208	310	101	)	)	PUNCT
eurjchem-208	310	102	.	.	PUNCT
eurjchem-208	311	1	the	the	DET
eurjchem-208	311	2	absorption	absorption	NOUN
eurjchem-208	311	3	bands	band	NOUN
eurjchem-208	311	4	of	of	ADP
eurjchem-208	311	5	nh	nh	PROPN
eurjchem-208	311	6	and	and	CCONJ
eurjchem-208	311	7	two	two	NUM
eurjchem-208	311	8	p	p	ADJ
eurjchem-208	311	9	=	=	NOUN
eurjchem-208	311	10	o	o	NOUN
eurjchem-208	311	11	groups	group	NOUN
eurjchem-208	311	12	in	in	ADP
eurjchem-208	311	13	ir	ir	PROPN
eurjchem-208	311	14	spectrum	spectrum	PROPN
eurjchem-208	311	15	appeared	appear	VERB
eurjchem-208	311	16	at	at	ADP
eurjchem-208	311	17	3300	3300	NUM
eurjchem-208	311	18	,	,	PUNCT
eurjchem-208	311	19	1287	1287	NUM
eurjchem-208	311	20	and	and	CCONJ
eurjchem-208	311	21	1233	1233	NUM
eurjchem-208	311	22	cm‐1	cm‐1	NOUN
eurjchem-208	311	23	,	,	PUNCT
eurjchem-208	311	24	respectively	respectively	ADV
eurjchem-208	311	25	.	.	PUNCT
eurjchem-208	312	1	also	also	ADV
eurjchem-208	312	2	,	,	PUNCT
eurjchem-208	312	3	the	the	DET
eurjchem-208	312	4	1h	1h	NUM
eurjchem-208	312	5	nmr	nmr	NOUN
eurjchem-208	312	6	spectrum	spectrum	NOUN
eurjchem-208	312	7	of	of	ADP
eurjchem-208	312	8	11	11	NUM
eurjchem-208	312	9	exhibited	exhibit	VERB
eurjchem-208	312	10	triplet	triplet	NOUN
eurjchem-208	312	11	and	and	CCONJ
eurjchem-208	312	12	quartet	quartet	NOUN
eurjchem-208	312	13	at	at	ADP
eurjchem-208	312	14			NUM
eurjchem-208	312	15	1.07	1.07	NUM
eurjchem-208	312	16	and	and	CCONJ
eurjchem-208	312	17	3.96	3.96	NUM
eurjchem-208	312	18	(	(	PUNCT
eurjchem-208	312	19	j=	j=	ADP
eurjchem-208	312	20	6.8	6.8	NUM
eurjchem-208	312	21	hz	hz	VERB
eurjchem-208	312	22	)	)	PUNCT
eurjchem-208	312	23	corresponding	correspond	VERB
eurjchem-208	312	24	to	to	ADP
eurjchem-208	312	25	ethoxy	ethoxy	ADJ
eurjchem-208	312	26	protons	proton	NOUN
eurjchem-208	312	27	.	.	PUNCT
eurjchem-208	313	1	because	because	SCONJ
eurjchem-208	313	2	of	of	ADP
eurjchem-208	313	3	coupling	couple	VERB
eurjchem-208	313	4	with	with	ADP
eurjchem-208	313	5	phosphorus	phosphorus	NOUN
eurjchem-208	313	6	atom	atom	NOUN
eurjchem-208	313	7	,	,	PUNCT
eurjchem-208	313	8	the	the	DET
eurjchem-208	313	9	proton	proton	NOUN
eurjchem-208	313	10	of	of	ADP
eurjchem-208	313	11	ch	ch	NOUN
eurjchem-208	313	12	–	–	PUNCT
eurjchem-208	313	13	p	p	PRON
eurjchem-208	313	14	exhibited	exhibit	VERB
eurjchem-208	313	15	a	a	DET
eurjchem-208	313	16	doublet	doublet	ADJ
eurjchem-208	313	17	signal	signal	NOUN
eurjchem-208	313	18	at	at	ADP
eurjchem-208	313	19			NUM
eurjchem-208	313	20	4.91	4.91	NUM
eurjchem-208	313	21	ppm	ppm	NOUN
eurjchem-208	313	22	(	(	PUNCT
eurjchem-208	313	23	jpch=	jpch=	PROPN
eurjchem-208	313	24	18.4	18.4	NUM
eurjchem-208	313	25	hz	hz	NOUN
eurjchem-208	313	26	)	)	PUNCT
eurjchem-208	313	27	.	.	PUNCT
eurjchem-208	314	1	moreover	moreover	ADV
eurjchem-208	314	2	,	,	PUNCT
eurjchem-208	314	3	its	its	PRON
eurjchem-208	314	4	13c	13c	NOUN
eurjchem-208	314	5	nmr	nmr	NOUN
eurjchem-208	314	6	spectrum	spectrum	NOUN
eurjchem-208	314	7	displayed	display	VERB
eurjchem-208	314	8	the	the	DET
eurjchem-208	314	9	ethoxy	ethoxy	ADJ
eurjchem-208	314	10	carbon	carbon	NOUN
eurjchem-208	314	11	atoms	atom	NOUN
eurjchem-208	314	12	at	at	ADP
eurjchem-208	314	13			NUM
eurjchem-208	314	14	16.0	16.0	NUM
eurjchem-208	314	15	and	and	CCONJ
eurjchem-208	314	16	62.7	62.7	NUM
eurjchem-208	314	17	ppm	ppm	NOUN
eurjchem-208	314	18	,	,	PUNCT
eurjchem-208	314	19	while	while	SCONJ
eurjchem-208	314	20	the	the	DET
eurjchem-208	314	21	carbon	carbon	NOUN
eurjchem-208	314	22	atom	atom	NOUN
eurjchem-208	314	23	of	of	ADP
eurjchem-208	314	24	ch	ch	NOUN
eurjchem-208	314	25	–	–	PUNCT
eurjchem-208	314	26	p	p	NOUN
eurjchem-208	314	27	at	at	ADP
eurjchem-208	314	28			NUM
eurjchem-208	314	29	46.1	46.1	NUM
eurjchem-208	314	30	ppm	ppm	NOUN
eurjchem-208	314	31	(	(	PUNCT
eurjchem-208	314	32	jpc=	jpc=	PROPN
eurjchem-208	314	33	161	161	NUM
eurjchem-208	314	34	hz	hz	NOUN
eurjchem-208	314	35	)	)	PUNCT
eurjchem-208	314	36	.	.	PUNCT
eurjchem-208	315	1	the	the	DET
eurjchem-208	315	2	presence	presence	NOUN
eurjchem-208	315	3	of	of	ADP
eurjchem-208	315	4	only	only	ADV
eurjchem-208	315	5	one	one	NUM
eurjchem-208	315	6	signal	signal	NOUN
eurjchem-208	315	7	observed	observe	VERB
eurjchem-208	315	8	for	for	ADP
eurjchem-208	315	9	ch	ch	NOUN
eurjchem-208	315	10	–	–	PUNCT
eurjchem-208	315	11	p	p	NOUN
eurjchem-208	315	12	and	and	CCONJ
eurjchem-208	315	13	och2ch3	och2ch3	ADJ
eurjchem-208	315	14	groups	group	NOUN
eurjchem-208	315	15	indicated	indicate	VERB
eurjchem-208	315	16	that	that	SCONJ
eurjchem-208	315	17	only	only	ADV
eurjchem-208	315	18	one	one	NUM
eurjchem-208	315	19	of	of	ADP
eurjchem-208	315	20	the	the	DET
eurjchem-208	315	21	two	two	NUM
eurjchem-208	315	22	possible	possible	ADJ
eurjchem-208	315	23	diastereomers	diastereomer	NOUN
eurjchem-208	315	24	(	(	PUNCT
eurjchem-208	315	25	meso	meso	NOUN
eurjchem-208	315	26	and	and	CCONJ
eurjchem-208	315	27	racemic	racemic	ADJ
eurjchem-208	315	28	forms	form	NOUN
eurjchem-208	315	29	)	)	PUNCT
eurjchem-208	315	30	is	be	AUX
eurjchem-208	315	31	formed	form	VERB
eurjchem-208	315	32	stereospecifically	stereospecifically	ADV
eurjchem-208	315	33	.	.	PUNCT
eurjchem-208	316	1	these	these	DET
eurjchem-208	316	2	observations	observation	NOUN
eurjchem-208	316	3	were	be	AUX
eurjchem-208	316	4	further	far	ADV
eurjchem-208	316	5	confirmed	confirm	VERB
eurjchem-208	316	6	by	by	ADP
eurjchem-208	316	7	analysis	analysis	NOUN
eurjchem-208	316	8	of	of	ADP
eurjchem-208	316	9	the	the	DET
eurjchem-208	316	10	31p	31p	NUM
eurjchem-208	316	11	nmr	nmr	NOUN
eurjchem-208	316	12	spectrum	spectrum	NOUN
eurjchem-208	316	13	of	of	ADP
eurjchem-208	316	14	11	11	NUM
eurjchem-208	316	15	,	,	PUNCT
eurjchem-208	316	16	in	in	ADP
eurjchem-208	316	17	which	which	PRON
eurjchem-208	316	18	only	only	ADV
eurjchem-208	316	19	one	one	NUM
eurjchem-208	316	20	sharp	sharp	ADJ
eurjchem-208	316	21	phosphorus	phosphorus	NOUN
eurjchem-208	316	22	signal	signal	NOUN
eurjchem-208	316	23	is	be	AUX
eurjchem-208	316	24	observed	observe	VERB
eurjchem-208	316	25	at	at	ADP
eurjchem-208	316	26			NUM
eurjchem-208	316	27	21.56	21.56	NUM
eurjchem-208	316	28	ppm	ppm	NOUN
eurjchem-208	316	29	for	for	ADP
eurjchem-208	316	30	‐aminophosphonate	‐aminophosphonate	ADJ
eurjchem-208	316	31	groups	group	NOUN
eurjchem-208	316	32	indicating	indicate	VERB
eurjchem-208	316	33	that	that	SCONJ
eurjchem-208	316	34	only	only	ADV
eurjchem-208	316	35	one	one	NUM
eurjchem-208	316	36	diastereomer	diastereomer	NOUN
eurjchem-208	316	37	contributes	contribute	VERB
eurjchem-208	316	38	to	to	ADP
eurjchem-208	316	39	the	the	DET
eurjchem-208	316	40	structure	structure	NOUN
eurjchem-208	316	41	[	[	X
eurjchem-208	316	42	41	41	NUM
eurjchem-208	316	43	]	]	PUNCT
eurjchem-208	316	44	.	.	PUNCT
eurjchem-208	317	1	recently	recently	ADV
eurjchem-208	317	2	,	,	PUNCT
eurjchem-208	317	3	chalcones	chalcone	NOUN
eurjchem-208	317	4	have	have	AUX
eurjchem-208	317	5	been	be	AUX
eurjchem-208	317	6	reported	report	VERB
eurjchem-208	317	7	to	to	PART
eurjchem-208	317	8	exhibit	exhibit	VERB
eurjchem-208	317	9	a	a	DET
eurjchem-208	317	10	wide	wide	ADJ
eurjchem-208	317	11	variety	variety	NOUN
eurjchem-208	317	12	of	of	ADP
eurjchem-208	317	13	pharmacological	pharmacological	ADJ
eurjchem-208	317	14	effects	effect	NOUN
eurjchem-208	317	15	[	[	X
eurjchem-208	317	16	42,43	42,43	X
eurjchem-208	317	17	]	]	PUNCT
eurjchem-208	317	18	.	.	PUNCT
eurjchem-208	318	1	thus	thus	ADV
eurjchem-208	318	2	,	,	PUNCT
eurjchem-208	318	3	when	when	SCONJ
eurjchem-208	318	4	bis(4‐	bis(4‐	PROPN
eurjchem-208	318	5	formylpyrazolyl)phosphine	formylpyrazolyl)phosphine	ADJ
eurjchem-208	318	6	oxide	oxide	NOUN
eurjchem-208	318	7	4a	4a	NOUN
eurjchem-208	318	8	was	be	AUX
eurjchem-208	318	9	allowed	allow	VERB
eurjchem-208	318	10	to	to	PART
eurjchem-208	318	11	react	react	VERB
eurjchem-208	318	12	with	with	ADP
eurjchem-208	318	13	phenacyltriphenylphosphonium	phenacyltriphenylphosphonium	NOUN
eurjchem-208	318	14	bromide	bromide	NOUN
eurjchem-208	318	15	in	in	ADP
eurjchem-208	318	16	dry	dry	ADJ
eurjchem-208	318	17	dioxane	dioxane	NOUN
eurjchem-208	318	18	containing	contain	VERB
eurjchem-208	318	19	drops	drop	NOUN
eurjchem-208	318	20	of	of	ADP
eurjchem-208	318	21	triethylamine	triethylamine	NOUN
eurjchem-208	318	22	as	as	ADP
eurjchem-208	318	23	basic	basic	ADJ
eurjchem-208	318	24	catalyst	catalyst	NOUN
eurjchem-208	318	25	under	under	ADP
eurjchem-208	318	26	wittig	wittig	NOUN
eurjchem-208	318	27	reaction	reaction	NOUN
eurjchem-208	318	28	conditions	condition	NOUN
eurjchem-208	318	29	[	[	X
eurjchem-208	318	30	44	44	NUM
eurjchem-208	318	31	]	]	PUNCT
eurjchem-208	318	32	,	,	PUNCT
eurjchem-208	318	33	afforded	afford	VERB
eurjchem-208	318	34	a	a	DET
eurjchem-208	318	35	product	product	NOUN
eurjchem-208	318	36	identified	identify	VERB
eurjchem-208	318	37	as	as	ADP
eurjchem-208	318	38	bis{3‐	bis{3‐	NOUN
eurjchem-208	318	39	phenyl‐4‐(1‐oxo‐1‐phenylprop‐2‐en‐3‐yl)‐1h‐pyrazol‐1‐yl	phenyl‐4‐(1‐oxo‐1‐phenylprop‐2‐en‐3‐yl)‐1h‐pyrazol‐1‐yl	NOUN
eurjchem-208	318	40	}	}	PUNCT
eurjchem-208	318	41	phosphine	phosphine	NOUN
eurjchem-208	318	42	oxide	oxide	NOUN
eurjchem-208	318	43	(	(	PUNCT
eurjchem-208	318	44	12	12	NUM
eurjchem-208	318	45	)	)	PUNCT
eurjchem-208	318	46	(	(	PUNCT
eurjchem-208	318	47	scheme10	scheme10	NOUN
eurjchem-208	318	48	)	)	PUNCT
eurjchem-208	318	49	.	.	PUNCT
eurjchem-208	319	1	the	the	DET
eurjchem-208	319	2	ir	ir	PROPN
eurjchem-208	319	3	spectrum	spectrum	NOUN
eurjchem-208	319	4	of	of	ADP
eurjchem-208	319	5	12	12	NUM
eurjchem-208	319	6	showed	show	VERB
eurjchem-208	319	7	one	one	NUM
eurjchem-208	319	8	characteristic	characteristic	ADJ
eurjchem-208	319	9	absorption	absorption	NOUN
eurjchem-208	319	10	band	band	NOUN
eurjchem-208	319	11	at	at	ADP
eurjchem-208	319	12	1687	1687	NUM
eurjchem-208	319	13	cm‐1	cm‐1	NOUN
eurjchem-208	319	14	assignable	assignable	ADJ
eurjchem-208	319	15	to	to	ADP
eurjchem-208	319	16	carbonyl	carbonyl	NOUN
eurjchem-208	319	17	groups	group	NOUN
eurjchem-208	319	18	.	.	PUNCT
eurjchem-208	320	1	also	also	ADV
eurjchem-208	320	2	,	,	PUNCT
eurjchem-208	320	3	its	its	PRON
eurjchem-208	320	4	1h	1h	NUM
eurjchem-208	320	5	nmr	nmr	NOUN
eurjchem-208	320	6	spectrum	spectrum	NOUN
eurjchem-208	320	7	exhibited	exhibit	VERB
eurjchem-208	320	8	two	two	NUM
eurjchem-208	320	9	doublet	doublet	ADJ
eurjchem-208	320	10	signals	signal	NOUN
eurjchem-208	320	11	at	at	ADP
eurjchem-208	320	12			NUM
eurjchem-208	320	13	7.78	7.78	NUM
eurjchem-208	320	14	and	and	CCONJ
eurjchem-208	320	15	8.09	8.09	NUM
eurjchem-208	320	16	ppm	ppm	NOUN
eurjchem-208	320	17	(	(	PUNCT
eurjchem-208	320	18	j=	j=	NOUN
eurjchem-208	320	19	13.8	13.8	NUM
eurjchem-208	320	20	hz	hz	VERB
eurjchem-208	320	21	)	)	PUNCT
eurjchem-208	320	22	due	due	ADP
eurjchem-208	320	23	to	to	ADP
eurjchem-208	320	24	olefinic	olefinic	ADJ
eurjchem-208	320	25	protons	proton	NOUN
eurjchem-208	320	26	h	h	NOUN
eurjchem-208	320	27	and	and	CCONJ
eurjchem-208	320	28	h	h	NOUN
eurjchem-208	320	29	,	,	PUNCT
eurjchem-208	320	30	respectively	respectively	ADV
eurjchem-208	320	31	,	,	PUNCT
eurjchem-208	320	32	while	while	SCONJ
eurjchem-208	320	33	the	the	DET
eurjchem-208	320	34	carbon	carbon	NOUN
eurjchem-208	320	35	atoms	atom	VERB
eurjchem-208	320	36	c	c	NOUN
eurjchem-208	320	37	and	and	CCONJ
eurjchem-208	320	38	cappeared	cappeare	VERB
eurjchem-208	320	39	at	at	ADP
eurjchem-208	320	40			NUM
eurjchem-208	320	41	118.7	118.7	NUM
eurjchem-208	320	42	and	and	CCONJ
eurjchem-208	320	43	138.0	138.0	NUM
eurjchem-208	320	44	ppm	ppm	NOUN
eurjchem-208	320	45	in	in	ADP
eurjchem-208	320	46	its	its	PRON
eurjchem-208	320	47	13c	13c	NOUN
eurjchem-208	320	48	nmr	nmr	NOUN
eurjchem-208	320	49	spectrum	spectrum	NOUN
eurjchem-208	320	50	[	[	X
eurjchem-208	320	51	45	45	NUM
eurjchem-208	320	52	]	]	PUNCT
eurjchem-208	320	53	.	.	PUNCT
eurjchem-208	321	1	moreover	moreover	ADV
eurjchem-208	321	2	,	,	PUNCT
eurjchem-208	321	3	the	the	DET
eurjchem-208	321	4	mass	mass	NOUN
eurjchem-208	321	5	spectrum	spectrum	NOUN
eurjchem-208	321	6	of	of	ADP
eurjchem-208	321	7	12	12	NUM
eurjchem-208	321	8	recorded	record	VERB
eurjchem-208	321	9	a	a	DET
eurjchem-208	321	10	highest	high	ADJ
eurjchem-208	321	11	ion	ion	NOUN
eurjchem-208	321	12	peak	peak	NOUN
eurjchem-208	321	13	at	at	ADP
eurjchem-208	321	14	m	m	PROPN
eurjchem-208	321	15	/	/	SYM
eurjchem-208	321	16	e	e	NOUN
eurjchem-208	321	17	414	414	NUM
eurjchem-208	321	18	after	after	ADP
eurjchem-208	321	19	losing	lose	VERB
eurjchem-208	321	20	diphenyl	diphenyl	NOUN
eurjchem-208	321	21	moieties	moiety	NOUN
eurjchem-208	321	22	and	and	CCONJ
eurjchem-208	321	23	carbon	carbon	NOUN
eurjchem-208	321	24	monoxide	monoxide	NOUN
eurjchem-208	321	25	with	with	ADP
eurjchem-208	321	26	a	a	DET
eurjchem-208	321	27	base	base	NOUN
eurjchem-208	321	28	peak	peak	NOUN
eurjchem-208	321	29	at	at	ADP
eurjchem-208	321	30	m	m	PROPN
eurjchem-208	321	31	/	/	SYM
eurjchem-208	321	32	e	e	PROPN
eurjchem-208	321	33	57	57	NUM
eurjchem-208	321	34	.	.	PUNCT
eurjchem-208	322	1	bis‐chalcone	bis‐chalcone	NOUN
eurjchem-208	322	2	12	12	NUM
eurjchem-208	322	3	is	be	AUX
eurjchem-208	322	4	seemed	seem	VERB
eurjchem-208	322	5	to	to	PART
eurjchem-208	322	6	be	be	AUX
eurjchem-208	322	7	a	a	DET
eurjchem-208	322	8	logical	logical	ADJ
eurjchem-208	322	9	starting	starting	NOUN
eurjchem-208	322	10	material	material	NOUN
eurjchem-208	322	11	for	for	ADP
eurjchem-208	322	12	synthesis	synthesis	NOUN
eurjchem-208	322	13	of	of	ADP
eurjchem-208	322	14	sulfur	sulfur	NOUN
eurjchem-208	322	15	and	and	CCONJ
eurjchem-208	322	16	phosphorus	phosphorus	NOUN
eurjchem-208	322	17	heterocyclesvia	heterocyclesvia	ADP
eurjchem-208	322	18	its	its	PRON
eurjchem-208	322	19	reaction	reaction	NOUN
eurjchem-208	322	20	with	with	ADP
eurjchem-208	322	21	sulfur	sulfur	NOUN
eurjchem-208	322	22	and	and	CCONJ
eurjchem-208	322	23	phosphorus	phosphorus	NOUN
eurjchem-208	322	24	nucleophiles	nucleophile	NOUN
eurjchem-208	322	25	.	.	PUNCT
eurjchem-208	323	1	thus	thus	ADV
eurjchem-208	323	2	,	,	PUNCT
eurjchem-208	323	3	reaction	reaction	NOUN
eurjchem-208	323	4	of	of	ADP
eurjchem-208	323	5	bis‐chalcone	bis‐chalcone	NOUN
eurjchem-208	323	6	12	12	NUM
eurjchem-208	323	7	with	with	ADP
eurjchem-208	323	8	thioglycolic	thioglycolic	ADJ
eurjchem-208	323	9	acid	acid	NOUN
eurjchem-208	323	10	in	in	ADP
eurjchem-208	323	11	dry	dry	ADJ
eurjchem-208	323	12	dioxane	dioxane	NOUN
eurjchem-208	323	13	containing	contain	VERB
eurjchem-208	323	14	anhydrous	anhydrous	ADJ
eurjchem-208	323	15	potassium	potassium	NOUN
eurjchem-208	323	16	carbonate	carbonate	NOUN
eurjchem-208	323	17	furnished	furnish	VERB
eurjchem-208	323	18	exclusively	exclusively	ADV
eurjchem-208	323	19	and	and	CCONJ
eurjchem-208	323	20	reasonable	reasonable	ADJ
eurjchem-208	323	21	good	good	ADJ
eurjchem-208	323	22	yield	yield	NOUN
eurjchem-208	323	23	a	a	DET
eurjchem-208	323	24	product	product	NOUN
eurjchem-208	323	25	that	that	PRON
eurjchem-208	323	26	could	could	AUX
eurjchem-208	323	27	be	be	AUX
eurjchem-208	323	28	formulated	formulate	VERB
eurjchem-208	323	29	as	as	ADP
eurjchem-208	323	30	bis{3‐phenyl‐4‐(4‐phenyl‐2‐thienyl)‐1h‐pyrazol‐	bis{3‐phenyl‐4‐(4‐phenyl‐2‐thienyl)‐1h‐pyrazol‐	NOUN
eurjchem-208	323	31	1‐yl}phosphine	1‐yl}phosphine	NUM
eurjchem-208	323	32	oxide	oxide	NOUN
eurjchem-208	323	33	(	(	PUNCT
eurjchem-208	323	34	14	14	NUM
eurjchem-208	323	35	)	)	PUNCT
eurjchem-208	323	36	(	(	PUNCT
eurjchem-208	323	37	scheme	scheme	NOUN
eurjchem-208	323	38	11	11	NUM
eurjchem-208	323	39	)	)	PUNCT
eurjchem-208	323	40	.	.	PUNCT
eurjchem-208	324	1	a	a	DET
eurjchem-208	324	2	plausible	plausible	ADJ
eurjchem-208	324	3	mechanism	mechanism	NOUN
eurjchem-208	324	4	involved	involve	VERB
eurjchem-208	324	5	an	an	DET
eurjchem-208	324	6	initial	initial	ADJ
eurjchem-208	324	7	michael	michael	PROPN
eurjchem-208	324	8	type	type	NOUN
eurjchem-208	324	9	addition	addition	NOUN
eurjchem-208	324	10	of	of	ADP
eurjchem-208	324	11	the	the	DET
eurjchem-208	324	12	thiol	thiol	ADJ
eurjchem-208	324	13	group	group	NOUN
eurjchem-208	324	14	of	of	ADP
eurjchem-208	324	15	thioglycolic	thioglycolic	ADJ
eurjchem-208	324	16	acid	acid	PROPN
eurjchem-208	324	17	to	to	ADP
eurjchem-208	324	18	the	the	DET
eurjchem-208	324	19	activated	activate	VERB
eurjchem-208	324	20	double	double	ADJ
eurjchem-208	324	21	bond	bond	NOUN
eurjchem-208	324	22	in	in	ADP
eurjchem-208	324	23	compound	compound	NOUN
eurjchem-208	324	24	12	12	NUM
eurjchem-208	324	25	,	,	PUNCT
eurjchem-208	324	26	followed	follow	VERB
eurjchem-208	324	27	by	by	ADP
eurjchem-208	324	28	cyclocondensation	cyclocondensation	NOUN
eurjchem-208	324	29	between	between	ADP
eurjchem-208	324	30	active	active	ADJ
eurjchem-208	324	31	methylene	methylene	NOUN
eurjchem-208	324	32	and	and	CCONJ
eurjchem-208	324	33	carbonyl	carbonyl	NOUN
eurjchem-208	324	34	group	group	NOUN
eurjchem-208	324	35	to	to	PART
eurjchem-208	324	36	give	give	VERB
eurjchem-208	324	37	the	the	DET
eurjchem-208	324	38	nonisolable	nonisolable	ADJ
eurjchem-208	324	39	intermediate	intermediate	ADJ
eurjchem-208	324	40	13	13	NUM
eurjchem-208	324	41	.	.	PUNCT
eurjchem-208	324	42	decarboxylation	decarboxylation	NOUN
eurjchem-208	324	43	and	and	CCONJ
eurjchem-208	324	44	auto‐oxidation	auto‐oxidation	NOUN
eurjchem-208	324	45	of	of	ADP
eurjchem-208	324	46	the	the	DET
eurjchem-208	324	47	intermediate	intermediate	ADJ
eurjchem-208	324	48	13	13	NUM
eurjchem-208	324	49	produced	produce	VERB
eurjchem-208	324	50	the	the	DET
eurjchem-208	324	51	final	final	ADJ
eurjchem-208	324	52	product	product	NOUN
eurjchem-208	324	53	14	14	NUM
eurjchem-208	324	54	(	(	PUNCT
eurjchem-208	324	55	scheme	scheme	NOUN
eurjchem-208	324	56	11	11	NUM
eurjchem-208	324	57	)	)	PUNCT
eurjchem-208	324	58	.	.	PUNCT
eurjchem-208	325	1	the	the	DET
eurjchem-208	325	2	chemical	chemical	ADJ
eurjchem-208	325	3	structure	structure	NOUN
eurjchem-208	325	4	of	of	ADP
eurjchem-208	325	5	14	14	NUM
eurjchem-208	325	6	was	be	AUX
eurjchem-208	325	7	elucidated	elucidate	VERB
eurjchem-208	325	8	on	on	ADP
eurjchem-208	325	9	the	the	DET
eurjchem-208	325	10	basis	basis	NOUN
eurjchem-208	325	11	of	of	ADP
eurjchem-208	325	12	spectral	spectral	ADJ
eurjchem-208	325	13	techniques	technique	NOUN
eurjchem-208	325	14	.	.	PUNCT
eurjchem-208	326	1	its	its	PRON
eurjchem-208	326	2	ir	ir	PROPN
eurjchem-208	326	3	spectrum	spectrum	NOUN
eurjchem-208	326	4	did	do	AUX
eurjchem-208	326	5	not	not	PART
eurjchem-208	326	6	record	record	VERB
eurjchem-208	326	7	any	any	DET
eurjchem-208	326	8	carbonyl	carbonyl	NOUN
eurjchem-208	326	9	or	or	CCONJ
eurjchem-208	326	10	hydroxyl	hydroxyl	NOUN
eurjchem-208	326	11	groups	group	NOUN
eurjchem-208	326	12	which	which	PRON
eurjchem-208	326	13	confirmed	confirm	VERB
eurjchem-208	326	14	the	the	DET
eurjchem-208	326	15	decarboxylation	decarboxylation	NOUN
eurjchem-208	326	16	process	process	NOUN
eurjchem-208	326	17	.	.	PUNCT
eurjchem-208	327	1	also	also	ADV
eurjchem-208	327	2	,	,	PUNCT
eurjchem-208	327	3	its	its	PRON
eurjchem-208	327	4	1hnmr	1hnmr	NUM
eurjchem-208	327	5	spectrum	spectrum	NOUN
eurjchem-208	327	6	displayed	display	VERB
eurjchem-208	327	7	resonated	resonate	VERB
eurjchem-208	327	8	signals	signal	NOUN
eurjchem-208	327	9	at	at	ADP
eurjchem-208	327	10			NUM
eurjchem-208	327	11	6.60	6.60	NUM
eurjchem-208	327	12	and	and	CCONJ
eurjchem-208	327	13	7.08	7.08	NUM
eurjchem-208	327	14	ppm	ppm	NOUN
eurjchem-208	327	15	due	due	ADP
eurjchem-208	327	16	to	to	ADP
eurjchem-208	327	17	the	the	DET
eurjchem-208	327	18	two	two	NUM
eurjchem-208	327	19	protons	proton	NOUN
eurjchem-208	327	20	c3	c3	NOUN
eurjchem-208	327	21	–	–	PUNCT
eurjchem-208	327	22	h	h	PROPN
eurjchem-208	327	23	and	and	CCONJ
eurjchem-208	327	24	c5	c5	PROPN
eurjchem-208	327	25	–	–	PUNCT
eurjchem-208	327	26	h	h	NOUN
eurjchem-208	327	27	of	of	ADP
eurjchem-208	327	28	thiophene	thiophene	NOUN
eurjchem-208	327	29	moieties	moiety	NOUN
eurjchem-208	327	30	,	,	PUNCT
eurjchem-208	327	31	respectively	respectively	ADV
eurjchem-208	327	32	,	,	PUNCT
eurjchem-208	327	33	in	in	ADP
eurjchem-208	327	34	addition	addition	NOUN
eurjchem-208	327	35	to	to	ADP
eurjchem-208	327	36	a	a	DET
eurjchem-208	327	37	doublet	doublet	ADJ
eurjchem-208	327	38	signal	signal	NOUN
eurjchem-208	327	39	at	at	ADP
eurjchem-208	327	40			NUM
eurjchem-208	327	41	7.64	7.64	NUM
eurjchem-208	327	42	ppm	ppm	NOUN
eurjchem-208	327	43	(	(	PUNCT
eurjchem-208	327	44	jph=594	jph=594	PROPN
eurjchem-208	327	45	hz	hz	NOUN
eurjchem-208	327	46	)	)	PUNCT
eurjchem-208	327	47	correspond	correspond	VERB
eurjchem-208	327	48	to	to	ADP
eurjchem-208	327	49	proton	proton	NOUN
eurjchem-208	327	50	of	of	ADP
eurjchem-208	327	51	h	h	NOUN
eurjchem-208	327	52	–	–	PUNCT
eurjchem-208	327	53	p	p	ADJ
eurjchem-208	327	54	=	=	NUM
eurjchem-208	327	55	o	o	NOUN
eurjchem-208	327	56	unit	unit	NOUN
eurjchem-208	327	57	.	.	PUNCT
eurjchem-208	328	1	scheme	scheme	NOUN
eurjchem-208	328	2	10	10	NUM
eurjchem-208	328	3	scheme	scheme	NOUN
eurjchem-208	328	4	11	11	NUM
eurjchem-208	328	5	moreover	moreover	ADV
eurjchem-208	328	6	,	,	PUNCT
eurjchem-208	328	7	it	it	PRON
eurjchem-208	328	8	has	have	AUX
eurjchem-208	328	9	been	be	AUX
eurjchem-208	328	10	found	find	VERB
eurjchem-208	328	11	that	that	SCONJ
eurjchem-208	328	12	the	the	DET
eurjchem-208	328	13	one‐pot	one‐pot	NOUN
eurjchem-208	328	14	reaction	reaction	NOUN
eurjchem-208	328	15	of	of	ADP
eurjchem-208	328	16	bis‐chalcone	bis‐chalcone	NOUN
eurjchem-208	328	17	12	12	NUM
eurjchem-208	328	18	with	with	ADP
eurjchem-208	328	19	diethyl	diethyl	NOUN
eurjchem-208	328	20	phosphite	phosphite	NOUN
eurjchem-208	328	21	in	in	ADP
eurjchem-208	328	22	the	the	DET
eurjchem-208	328	23	presence	presence	NOUN
eurjchem-208	328	24	of	of	ADP
eurjchem-208	328	25	bf3.et2o	bf3.et2o	PROPN
eurjchem-208	328	26	at	at	ADP
eurjchem-208	328	27	80	80	NUM
eurjchem-208	328	28	oc	oc	NOUN
eurjchem-208	328	29	for	for	ADP
eurjchem-208	328	30	8	8	NUM
eurjchem-208	328	31	hours	hour	NOUN
eurjchem-208	328	32	,	,	PUNCT
eurjchem-208	328	33	afforded	afford	VERB
eurjchem-208	328	34	bis{[2‐ethoxy‐2‐oxo‐5‐	bis{[2‐ethoxy‐2‐oxo‐5‐	PROPN
eurjchem-208	328	35	phenyl‐2,3‐dihydro‐1,2‐oxaphosphol‐3‐yl]‐3‐phenyl‐1h‐pyra‐	phenyl‐2,3‐dihydro‐1,2‐oxaphosphol‐3‐yl]‐3‐phenyl‐1h‐pyra‐	ADP
eurjchem-208	328	36	zol‐1‐yl}phosphine	zol‐1‐yl}phosphine	ADJ
eurjchem-208	328	37	oxide	oxide	NOUN
eurjchem-208	328	38	(	(	PUNCT
eurjchem-208	328	39	16	16	NUM
eurjchem-208	328	40	)	)	PUNCT
eurjchem-208	328	41	(	(	PUNCT
eurjchem-208	328	42	scheme	scheme	NOUN
eurjchem-208	328	43	12	12	NUM
eurjchem-208	328	44	)	)	PUNCT
eurjchem-208	328	45	.	.	PUNCT
eurjchem-208	329	1	the	the	DET
eurjchem-208	329	2	proposed	propose	VERB
eurjchem-208	329	3	mechanism	mechanism	NOUN
eurjchem-208	329	4	involved	involve	VERB
eurjchem-208	329	5	an	an	DET
eurjchem-208	329	6	initial	initial	ADJ
eurjchem-208	329	7	michael	michael	PROPN
eurjchem-208	329	8	type	type	NOUN
eurjchem-208	329	9	addition	addition	NOUN
eurjchem-208	329	10	of	of	ADP
eurjchem-208	329	11	phosphorus	phosphorus	NOUN
eurjchem-208	329	12	atom	atom	NOUN
eurjchem-208	329	13	of	of	ADP
eurjchem-208	329	14	diethyl	diethyl	NOUN
eurjchem-208	329	15	phosphite	phosphite	NOUN
eurjchem-208	329	16	to	to	ADP
eurjchem-208	329	17	the	the	DET
eurjchem-208	329	18	activated	activate	VERB
eurjchem-208	329	19	double	double	ADJ
eurjchem-208	329	20	bond	bond	NOUN
eurjchem-208	329	21	in	in	ADP
eurjchem-208	329	22	compound	compound	NOUN
eurjchem-208	329	23	12	12	NUM
eurjchem-208	329	24	to	to	PART
eurjchem-208	329	25	give	give	VERB
eurjchem-208	329	26	the	the	DET
eurjchem-208	329	27	nonisolable	nonisolable	ADJ
eurjchem-208	329	28	intermediate	intermediate	ADJ
eurjchem-208	329	29	15	15	NUM
eurjchem-208	329	30	,	,	PUNCT
eurjchem-208	329	31	which	which	DET
eurjchem-208	329	32	underwent	undergo	VERB
eurjchem-208	329	33	cyclization	cyclization	NOUN
eurjchem-208	329	34	by	by	ADP
eurjchem-208	329	35	elimination	elimination	NOUN
eurjchem-208	329	36	of	of	ADP
eurjchem-208	329	37	ethanol	ethanol	NOUN
eurjchem-208	329	38	molecules	molecule	NOUN
eurjchem-208	329	39	to	to	PART
eurjchem-208	329	40	give	give	VERB
eurjchem-208	329	41	16	16	NUM
eurjchem-208	329	42	(	(	PUNCT
eurjchem-208	329	43	scheme	scheme	NOUN
eurjchem-208	329	44	12	12	NUM
eurjchem-208	329	45	)	)	PUNCT
eurjchem-208	330	1	[	[	X
eurjchem-208	330	2	46	46	NUM
eurjchem-208	330	3	]	]	PUNCT
eurjchem-208	330	4	.	.	PUNCT
eurjchem-208	331	1	the	the	DET
eurjchem-208	331	2	1h	1h	NUM
eurjchem-208	331	3	nmr	nmr	NOUN
eurjchem-208	331	4	spectrum	spectrum	NOUN
eurjchem-208	331	5	of	of	ADP
eurjchem-208	331	6	16	16	NUM
eurjchem-208	331	7	displayed	display	VERB
eurjchem-208	331	8	two	two	NUM
eurjchem-208	331	9	doublet	doublet	ADJ
eurjchem-208	331	10	signals	signal	NOUN
eurjchem-208	331	11	at	at	ADP
eurjchem-208	331	12			NUM
eurjchem-208	331	13	6.70	6.70	NUM
eurjchem-208	331	14	ppm	ppm	NOUN
eurjchem-208	331	15	(	(	PUNCT
eurjchem-208	331	16	j=	j=	PROPN
eurjchem-208	331	17	28	28	NUM
eurjchem-208	331	18	hz	hz	VERB
eurjchem-208	331	19	)	)	PUNCT
eurjchem-208	331	20	and	and	CCONJ
eurjchem-208	331	21	7.15	7.15	NUM
eurjchem-208	331	22	ppm	ppm	NOUN
eurjchem-208	331	23	(	(	PUNCT
eurjchem-208	331	24	j=	j=	ADP
eurjchem-208	331	25	5	5	NUM
eurjchem-208	331	26	hz	hz	ADJ
eurjchem-208	331	27	)	)	PUNCT
eurjchem-208	331	28	assignable	assignable	ADJ
eurjchem-208	331	29	to	to	ADP
eurjchem-208	331	30	protons	proton	NOUN
eurjchem-208	331	31	of	of	ADP
eurjchem-208	331	32	ch	ch	NOUN
eurjchem-208	331	33	–	–	PUNCT
eurjchem-208	331	34	p	p	NOUN
eurjchem-208	331	35	and	and	CCONJ
eurjchem-208	331	36	c4	c4	NOUN
eurjchem-208	331	37	–	–	PUNCT
eurjchem-208	331	38	h	h	NOUN
eurjchem-208	331	39	,	,	PUNCT
eurjchem-208	331	40	respectively	respectively	ADV
eurjchem-208	331	41	,	,	PUNCT
eurjchem-208	331	42	of	of	ADP
eurjchem-208	331	43	oxaphosphole	oxaphosphole	ADJ
eurjchem-208	331	44	rings	ring	NOUN
eurjchem-208	331	45	,	,	PUNCT
eurjchem-208	331	46	in	in	ADP
eurjchem-208	331	47	addition	addition	NOUN
eurjchem-208	331	48	to	to	ADP
eurjchem-208	331	49	the	the	DET
eurjchem-208	331	50	presence	presence	NOUN
eurjchem-208	331	51	of	of	ADP
eurjchem-208	331	52	the	the	DET
eurjchem-208	331	53	ethoxy	ethoxy	ADJ
eurjchem-208	331	54	protons	proton	NOUN
eurjchem-208	331	55	as	as	ADP
eurjchem-208	331	56	triplet	triplet	NOUN
eurjchem-208	331	57	and	and	CCONJ
eurjchem-208	331	58	quartet	quartet	NOUN
eurjchem-208	331	59	at	at	ADP
eurjchem-208	331	60			NUM
eurjchem-208	331	61	1.34	1.34	NUM
eurjchem-208	331	62	and	and	CCONJ
eurjchem-208	331	63	4.35	4.35	NUM
eurjchem-208	331	64	ppm	ppm	NOUN
eurjchem-208	331	65	(	(	PUNCT
eurjchem-208	331	66	j=	j=	NOUN
eurjchem-208	331	67	7.2	7.2	NUM
eurjchem-208	331	68	hz	hz	NOUN
eurjchem-208	331	69	)	)	PUNCT
eurjchem-208	331	70	,	,	PUNCT
eurjchem-208	331	71	respectively	respectively	ADV
eurjchem-208	331	72	.	.	PUNCT
eurjchem-208	332	1	also	also	ADV
eurjchem-208	332	2	,	,	PUNCT
eurjchem-208	332	3	its	its	PRON
eurjchem-208	332	4	ir	ir	PROPN
eurjchem-208	332	5	spectrum	spectrum	NOUN
eurjchem-208	332	6	confirmed	confirm	VERB
eurjchem-208	332	7	32	32	NUM
eurjchem-208	332	8	abdel‐aziz	abdel‐aziz	NOUN
eurjchem-208	332	9	et	et	PROPN
eurjchem-208	332	10	al	al	PROPN
eurjchem-208	332	11	.	.	PUNCT
eurjchem-208	332	12	/	/	SYM
eurjchem-208	332	13	european	european	PROPN
eurjchem-208	332	14	journal	journal	PROPN
eurjchem-208	332	15	of	of	ADP
eurjchem-208	332	16	chemistry	chemistry	NOUN
eurjchem-208	332	17	2	2	NUM
eurjchem-208	332	18	(	(	PUNCT
eurjchem-208	332	19	1	1	NUM
eurjchem-208	332	20	)	)	PUNCT
eurjchem-208	332	21	(	(	PUNCT
eurjchem-208	332	22	2011	2011	NUM
eurjchem-208	332	23	)	)	PUNCT
eurjchem-208	332	24	25‐35	25‐35	NUM
eurjchem-208	332	25	the	the	DET
eurjchem-208	332	26	disappearance	disappearance	NOUN
eurjchem-208	332	27	of	of	ADP
eurjchem-208	332	28	carbonyl	carbonyl	NOUN
eurjchem-208	332	29	group	group	NOUN
eurjchem-208	332	30	of	of	ADP
eurjchem-208	332	31	compound	compound	NOUN
eurjchem-208	332	32	12	12	NUM
eurjchem-208	332	33	which	which	PRON
eurjchem-208	332	34	support	support	VERB
eurjchem-208	332	35	the	the	DET
eurjchem-208	332	36	cyclized	cyclized	ADJ
eurjchem-208	332	37	state	state	NOUN
eurjchem-208	332	38	.	.	PUNCT
eurjchem-208	333	1	n	n	CCONJ
eurjchem-208	333	2	n	n	CCONJ
eurjchem-208	333	3	p	p	NOUN
eurjchem-208	333	4	n	n	CCONJ
eurjchem-208	333	5	n	n	NOUN
eurjchem-208	333	6	h	h	NOUN
eurjchem-208	334	1	o	o	NOUN
eurjchem-208	334	2	phph	phph	INTJ
eurjchem-208	334	3	o	o	INTJ
eurjchem-208	334	4	o	o	X
eurjchem-208	334	5	ph	ph	NOUN
eurjchem-208	334	6	ph	ph	PROPN
eurjchem-208	334	7	12	12	NUM
eurjchem-208	334	8	h	h	NOUN
eurjchem-208	334	9	-	-	PUNCT
eurjchem-208	334	10	p(o)(oet)2	p(o)(oet)2	NOUN
eurjchem-208	334	11	bf3.et2o	bf3.et2o	PROPN
eurjchem-208	334	12	o	o	PROPN
eurjchem-208	334	13	p	p	PROPN
eurjchem-208	334	14	h	h	NOUN
eurjchem-208	334	15	oph	oph	PROPN
eurjchem-208	334	16	oet	oet	ADJ
eurjchem-208	335	1	o	o	PROPN
eurjchem-208	336	1	p	p	NOUN
eurjchem-208	336	2	h	h	NOUN
eurjchem-208	336	3	o	o	NOUN
eurjchem-208	336	4	ph	ph	NOUN
eurjchem-208	336	5	oet	oet	VERB
eurjchem-208	336	6	n	n	CCONJ
eurjchem-208	336	7	n	n	PRON
eurjchem-208	336	8	p	p	NOUN
eurjchem-208	336	9	n	n	CCONJ
eurjchem-208	336	10	n	n	NOUN
eurjchem-208	336	11	h	h	NOUN
eurjchem-208	337	1	o	o	NOUN
eurjchem-208	337	2	phph	phph	NOUN
eurjchem-208	337	3	16	16	NUM
eurjchem-208	337	4	n	n	CCONJ
eurjchem-208	337	5	n	n	PROPN
eurjchem-208	337	6	p	p	NOUN
eurjchem-208	337	7	n	n	CCONJ
eurjchem-208	337	8	n	n	NOUN
eurjchem-208	337	9	h	h	NOUN
eurjchem-208	338	1	o	o	NOUN
eurjchem-208	338	2	phph	phph	NOUN
eurjchem-208	339	1	p	p	NOUN
eurjchem-208	339	2	o	o	NOUN
eurjchem-208	339	3	h	h	NOUN
eurjchem-208	340	1	p	p	NOUN
eurjchem-208	341	1	o	o	INTJ
eurjchem-208	342	1	h	h	NOUN
eurjchem-208	343	1	oet	oet	VERB
eurjchem-208	343	2	etooeteto	etooeteto	VERB
eurjchem-208	343	3	ho	ho	PROPN
eurjchem-208	344	1	oh	oh	INTJ
eurjchem-208	344	2	phph	phph	NOUN
eurjchem-208	344	3	15	15	NUM
eurjchem-208	344	4	2	2	NUM
eurjchem-208	344	5	etoh82	etoh82	NOUN
eurjchem-208	344	6	%	%	NOUN
eurjchem-208	344	7	scheme	scheme	NOUN
eurjchem-208	344	8	12	12	NUM
eurjchem-208	344	9	reaction	reaction	NOUN
eurjchem-208	344	10	of	of	ADP
eurjchem-208	344	11	bis(4‐formylpyrazolyl)phosphine	bis(4‐formylpyrazolyl)phosphine	PROPN
eurjchem-208	344	12	oxide	oxide	NOUN
eurjchem-208	344	13	4b	4b	NOUN
eurjchem-208	344	14	with	with	ADP
eurjchem-208	344	15	4‐phenylthiosemicarbazide	4‐phenylthiosemicarbazide	PROPN
eurjchem-208	344	16	(	(	PUNCT
eurjchem-208	344	17	17	17	NUM
eurjchem-208	344	18	)	)	PUNCT
eurjchem-208	344	19	in	in	ADP
eurjchem-208	344	20	refluxing	refluxing	NOUN
eurjchem-208	344	21	ethanol	ethanol	NOUN
eurjchem-208	344	22	produced	produce	VERB
eurjchem-208	344	23	the	the	DET
eurjchem-208	344	24	corresponding	correspond	VERB
eurjchem-208	344	25	bis‐thiosemicarbazone	bis‐thiosemicarbazone	NOUN
eurjchem-208	344	26	18	18	NUM
eurjchem-208	344	27	in	in	ADP
eurjchem-208	344	28	moderate	moderate	ADJ
eurjchem-208	344	29	yield	yield	NOUN
eurjchem-208	344	30	(	(	PUNCT
eurjchem-208	344	31	scheme	scheme	NOUN
eurjchem-208	344	32	13	13	NUM
eurjchem-208	344	33	)	)	PUNCT
eurjchem-208	344	34	.	.	PUNCT
eurjchem-208	345	1	the	the	DET
eurjchem-208	345	2	structure	structure	NOUN
eurjchem-208	345	3	of	of	ADP
eurjchem-208	345	4	18	18	NUM
eurjchem-208	345	5	was	be	AUX
eurjchem-208	345	6	established	establish	VERB
eurjchem-208	345	7	on	on	ADP
eurjchem-208	345	8	the	the	DET
eurjchem-208	345	9	basis	basis	NOUN
eurjchem-208	345	10	of	of	ADP
eurjchem-208	345	11	its	its	PRON
eurjchem-208	345	12	elemental	elemental	ADJ
eurjchem-208	345	13	analysis	analysis	NOUN
eurjchem-208	345	14	,	,	PUNCT
eurjchem-208	345	15	ir	ir	INTJ
eurjchem-208	345	16	,	,	PUNCT
eurjchem-208	345	17	1h	1h	NUM
eurjchem-208	345	18	nmr	nmr	NOUN
eurjchem-208	345	19	and	and	CCONJ
eurjchem-208	345	20	mass	mass	ADJ
eurjchem-208	345	21	spectral	spectral	ADJ
eurjchem-208	345	22	data	datum	NOUN
eurjchem-208	345	23	(	(	PUNCT
eurjchem-208	345	24	see	see	VERB
eurjchem-208	345	25	experimental	experimental	ADJ
eurjchem-208	345	26	section	section	NOUN
eurjchem-208	345	27	)	)	PUNCT
eurjchem-208	345	28	.	.	PUNCT
eurjchem-208	346	1	scheme	scheme	NOUN
eurjchem-208	346	2	13	13	NUM
eurjchem-208	346	3	it	it	PRON
eurjchem-208	346	4	is	be	AUX
eurjchem-208	346	5	known	know	VERB
eurjchem-208	346	6	that	that	SCONJ
eurjchem-208	346	7	thiosemicarbazones	thiosemicarbazone	NOUN
eurjchem-208	346	8	could	could	AUX
eurjchem-208	346	9	be	be	AUX
eurjchem-208	346	10	used	use	VERB
eurjchem-208	346	11	as	as	ADP
eurjchem-208	346	12	a	a	DET
eurjchem-208	346	13	precursor	precursor	NOUN
eurjchem-208	346	14	for	for	ADP
eurjchem-208	346	15	the	the	DET
eurjchem-208	346	16	synthesis	synthesis	NOUN
eurjchem-208	346	17	of	of	ADP
eurjchem-208	346	18	a	a	DET
eurjchem-208	346	19	variety	variety	NOUN
eurjchem-208	346	20	of	of	ADP
eurjchem-208	346	21	bioactive	bioactive	PROPN
eurjchem-208	346	22	sulfur‐	sulfur‐	NOUN
eurjchem-208	346	23	nitrogen	nitrogen	PROPN
eurjchem-208	346	24	heterocyclic	heterocyclic	PROPN
eurjchem-208	346	25	systems	system	NOUN
eurjchem-208	347	1	[	[	X
eurjchem-208	347	2	47,48	47,48	NOUN
eurjchem-208	347	3	]	]	X
eurjchem-208	347	4	.	.	PUNCT
eurjchem-208	348	1	thus	thus	ADV
eurjchem-208	348	2	,	,	PUNCT
eurjchem-208	348	3	refluxing	refluxing	NOUN
eurjchem-208	348	4	of	of	ADP
eurjchem-208	348	5	bis‐	bis‐	PROPN
eurjchem-208	348	6	thiosemicarbazone	thiosemicarbazone	NOUN
eurjchem-208	348	7	18	18	NUM
eurjchem-208	348	8	in	in	ADP
eurjchem-208	348	9	acetic	acetic	ADJ
eurjchem-208	348	10	anhydride	anhydride	NOUN
eurjchem-208	348	11	for	for	ADP
eurjchem-208	348	12	4	4	NUM
eurjchem-208	348	13	hours	hour	NOUN
eurjchem-208	348	14	produced	produce	VERB
eurjchem-208	348	15	the	the	DET
eurjchem-208	348	16	corresponding	corresponding	ADJ
eurjchem-208	348	17	bis(thiadiazolylpyrazolyl)phosphine	bis(thiadiazolylpyrazolyl)phosphine	NUM
eurjchem-208	348	18	oxide	oxide	NOUN
eurjchem-208	348	19	20	20	NUM
eurjchem-208	348	20	in	in	ADP
eurjchem-208	348	21	56	56	NUM
eurjchem-208	348	22	%	%	NOUN
eurjchem-208	348	23	yield	yield	NOUN
eurjchem-208	348	24	(	(	PUNCT
eurjchem-208	348	25	scheme	scheme	NOUN
eurjchem-208	348	26	14	14	NUM
eurjchem-208	348	27	)	)	PUNCT
eurjchem-208	348	28	.	.	PUNCT
eurjchem-208	349	1	the	the	DET
eurjchem-208	349	2	formation	formation	NOUN
eurjchem-208	349	3	of	of	ADP
eurjchem-208	349	4	20	20	NUM
eurjchem-208	349	5	may	may	AUX
eurjchem-208	349	6	be	be	AUX
eurjchem-208	349	7	occurred	occur	VERB
eurjchem-208	349	8	via	via	ADP
eurjchem-208	349	9	acetylation	acetylation	NOUN
eurjchem-208	349	10	of	of	ADP
eurjchem-208	349	11	nhph	nhph	ADJ
eurjchem-208	349	12	moieties	moiety	NOUN
eurjchem-208	349	13	and	and	CCONJ
eurjchem-208	349	14	the	the	DET
eurjchem-208	349	15	azomethine‐	azomethine‐	PROPN
eurjchem-208	349	16	nitrogen	nitrogen	NOUN
eurjchem-208	349	17	atoms	atom	NOUN
eurjchem-208	349	18	which	which	PRON
eurjchem-208	349	19	favor	favor	VERB
eurjchem-208	349	20	the	the	DET
eurjchem-208	349	21	development	development	NOUN
eurjchem-208	349	22	of	of	ADP
eurjchem-208	349	23	a	a	DET
eurjchem-208	349	24	positive	positive	ADJ
eurjchem-208	349	25	charge	charge	NOUN
eurjchem-208	349	26	on	on	ADP
eurjchem-208	349	27	the	the	DET
eurjchem-208	349	28	carbon	carbon	NOUN
eurjchem-208	349	29	atoms	atom	NOUN
eurjchem-208	349	30	of	of	ADP
eurjchem-208	349	31	these	these	DET
eurjchem-208	349	32	groups	group	NOUN
eurjchem-208	349	33	to	to	PART
eurjchem-208	349	34	give	give	VERB
eurjchem-208	349	35	the	the	DET
eurjchem-208	349	36	intermediate	intermediate	ADJ
eurjchem-208	349	37	19	19	NUM
eurjchem-208	349	38	,	,	PUNCT
eurjchem-208	349	39	which	which	DET
eurjchem-208	349	40	underwent	undergo	VERB
eurjchem-208	349	41	ring	ring	NOUN
eurjchem-208	349	42	closure	closure	NOUN
eurjchem-208	349	43	by	by	ADP
eurjchem-208	349	44	attack	attack	NOUN
eurjchem-208	349	45	of	of	ADP
eurjchem-208	349	46	sulfur	sulfur	NOUN
eurjchem-208	349	47	atom	atom	NOUN
eurjchem-208	349	48	to	to	PART
eurjchem-208	349	49	eliminate	eliminate	VERB
eurjchem-208	349	50	two	two	NUM
eurjchem-208	349	51	molecules	molecule	NOUN
eurjchem-208	349	52	of	of	ADP
eurjchem-208	349	53	acetic	acetic	ADJ
eurjchem-208	349	54	acid	acid	NOUN
eurjchem-208	349	55	to	to	PART
eurjchem-208	349	56	give	give	VERB
eurjchem-208	349	57	the	the	DET
eurjchem-208	349	58	final	final	ADJ
eurjchem-208	349	59	product	product	NOUN
eurjchem-208	349	60	20	20	NUM
eurjchem-208	349	61	(	(	PUNCT
eurjchem-208	349	62	scheme	scheme	NOUN
eurjchem-208	349	63	14	14	NUM
eurjchem-208	349	64	)	)	PUNCT
eurjchem-208	350	1	[	[	X
eurjchem-208	350	2	49	49	NUM
eurjchem-208	350	3	]	]	PUNCT
eurjchem-208	350	4	.	.	PUNCT
eurjchem-208	351	1	the	the	DET
eurjchem-208	351	2	structure	structure	NOUN
eurjchem-208	351	3	of	of	ADP
eurjchem-208	351	4	20	20	NUM
eurjchem-208	351	5	was	be	AUX
eurjchem-208	351	6	established	establish	VERB
eurjchem-208	351	7	on	on	ADP
eurjchem-208	351	8	the	the	DET
eurjchem-208	351	9	basis	basis	NOUN
eurjchem-208	351	10	of	of	ADP
eurjchem-208	351	11	spectral	spectral	ADJ
eurjchem-208	351	12	data	datum	NOUN
eurjchem-208	351	13	.	.	PUNCT
eurjchem-208	352	1	its	its	PRON
eurjchem-208	352	2	ir	ir	PROPN
eurjchem-208	352	3	spectrum	spectrum	NOUN
eurjchem-208	352	4	confirmed	confirm	VERB
eurjchem-208	352	5	the	the	DET
eurjchem-208	352	6	presence	presence	NOUN
eurjchem-208	352	7	of	of	ADP
eurjchem-208	352	8	c	c	NOUN
eurjchem-208	352	9	=	=	NOUN
eurjchem-208	352	10	o	o	NOUN
eurjchem-208	352	11	of	of	ADP
eurjchem-208	352	12	acetyl	acetyl	NOUN
eurjchem-208	352	13	groups	group	NOUN
eurjchem-208	352	14	at	at	ADP
eurjchem-208	352	15	1688	1688	NUM
eurjchem-208	352	16	and	and	CCONJ
eurjchem-208	352	17	1667	1667	NUM
eurjchem-208	352	18	cm‐1	cm‐1	NOUN
eurjchem-208	352	19	,	,	PUNCT
eurjchem-208	352	20	while	while	SCONJ
eurjchem-208	352	21	its	its	PRON
eurjchem-208	352	22	1h	1h	NUM
eurjchem-208	352	23	nmr	nmr	NOUN
eurjchem-208	352	24	spectrum	spectrum	NOUN
eurjchem-208	352	25	revealed	reveal	VERB
eurjchem-208	352	26	two	two	NUM
eurjchem-208	352	27	singlet	singlet	ADJ
eurjchem-208	352	28	signals	signal	NOUN
eurjchem-208	352	29	at	at	ADP
eurjchem-208	352	30			NUM
eurjchem-208	352	31	1.81	1.81	NUM
eurjchem-208	352	32	and	and	CCONJ
eurjchem-208	352	33	1.88	1.88	NUM
eurjchem-208	352	34	ppm	ppm	NOUN
eurjchem-208	352	35	assigned	assign	VERB
eurjchem-208	352	36	to	to	ADP
eurjchem-208	352	37	protons	proton	NOUN
eurjchem-208	352	38	of	of	ADP
eurjchem-208	352	39	methyl	methyl	NOUN
eurjchem-208	352	40	groups	group	NOUN
eurjchem-208	352	41	,	,	PUNCT
eurjchem-208	352	42	in	in	ADP
eurjchem-208	352	43	addition	addition	NOUN
eurjchem-208	352	44	to	to	ADP
eurjchem-208	352	45	singlet	singlet	ADJ
eurjchem-208	352	46	signal	signal	NOUN
eurjchem-208	352	47	at	at	ADP
eurjchem-208	352	48			NUM
eurjchem-208	352	49	6.54	6.54	NUM
eurjchem-208	352	50	ppm	ppm	NOUN
eurjchem-208	352	51	due	due	ADP
eurjchem-208	352	52	to	to	ADP
eurjchem-208	352	53	c5	c5	PROPN
eurjchem-208	352	54	–	–	PUNCT
eurjchem-208	352	55	h	h	NOUN
eurjchem-208	352	56	of	of	ADP
eurjchem-208	352	57	thiadiazole	thiadiazole	NOUN
eurjchem-208	352	58	moieties	moiety	NOUN
eurjchem-208	352	59	.	.	PUNCT
eurjchem-208	353	1	the	the	DET
eurjchem-208	353	2	13c	13c	NUM
eurjchem-208	353	3	nmr	nmr	NOUN
eurjchem-208	353	4	spectrum	spectrum	NOUN
eurjchem-208	353	5	of	of	ADP
eurjchem-208	353	6	20	20	NUM
eurjchem-208	353	7	was	be	AUX
eurjchem-208	353	8	also	also	ADV
eurjchem-208	353	9	good	good	ADJ
eurjchem-208	353	10	support	support	NOUN
eurjchem-208	353	11	for	for	ADP
eurjchem-208	353	12	the	the	DET
eurjchem-208	353	13	proposed	propose	VERB
eurjchem-208	353	14	structure	structure	NOUN
eurjchem-208	353	15	which	which	PRON
eurjchem-208	353	16	exhibited	exhibit	VERB
eurjchem-208	353	17	characteristic	characteristic	ADJ
eurjchem-208	353	18	signals	signal	NOUN
eurjchem-208	353	19	at	at	ADP
eurjchem-208	353	20			NUM
eurjchem-208	353	21	21.0	21.0	NUM
eurjchem-208	353	22	,	,	PUNCT
eurjchem-208	353	23	23.1	23.1	NUM
eurjchem-208	353	24	,	,	PUNCT
eurjchem-208	353	25	60.4	60.4	NUM
eurjchem-208	353	26	and	and	CCONJ
eurjchem-208	353	27	153.0	153.0	NUM
eurjchem-208	353	28	ppm	ppm	NOUN
eurjchem-208	353	29	corresponding	correspond	VERB
eurjchem-208	353	30	to	to	ADP
eurjchem-208	353	31	carbon	carbon	NOUN
eurjchem-208	353	32	atoms	atom	NOUN
eurjchem-208	353	33	of	of	ADP
eurjchem-208	353	34	two	two	NUM
eurjchem-208	353	35	methyl	methyl	NOUN
eurjchem-208	353	36	groups	group	NOUN
eurjchem-208	353	37	,	,	PUNCT
eurjchem-208	353	38	c–5	c–5	NOUN
eurjchem-208	353	39	and	and	CCONJ
eurjchem-208	353	40	c–2	c–2	NOUN
eurjchem-208	353	41	of	of	ADP
eurjchem-208	353	42	thiadiazole	thiadiazole	NOUN
eurjchem-208	353	43	moieties	moiety	NOUN
eurjchem-208	353	44	,	,	PUNCT
eurjchem-208	353	45	respectively	respectively	ADV
eurjchem-208	353	46	.	.	PUNCT
eurjchem-208	354	1	also	also	ADV
eurjchem-208	354	2	,	,	PUNCT
eurjchem-208	354	3	the	the	DET
eurjchem-208	354	4	carbon	carbon	NOUN
eurjchem-208	354	5	atoms	atom	NOUN
eurjchem-208	354	6	of	of	ADP
eurjchem-208	354	7	carbonyl	carbonyl	NOUN
eurjchem-208	354	8	groups	group	NOUN
eurjchem-208	354	9	appeared	appear	VERB
eurjchem-208	354	10	at	at	ADP
eurjchem-208	354	11			NUM
eurjchem-208	354	12	168.0	168.0	NUM
eurjchem-208	354	13	and	and	CCONJ
eurjchem-208	354	14	170.1	170.1	NUM
eurjchem-208	354	15	ppm	ppm	NOUN
eurjchem-208	354	16	.	.	PUNCT
eurjchem-208	355	1	scheme	scheme	NOUN
eurjchem-208	355	2	14	14	NUM
eurjchem-208	355	3	finally	finally	ADV
eurjchem-208	355	4	,	,	PUNCT
eurjchem-208	355	5	heterocyclization	heterocyclization	NOUN
eurjchem-208	355	6	of	of	ADP
eurjchem-208	355	7	bis‐thiosemicarbazone	bis‐thiosemicarbazone	PROPN
eurjchem-208	355	8	18	18	NUM
eurjchem-208	355	9	with	with	ADP
eurjchem-208	355	10	diethyl	diethyl	NOUN
eurjchem-208	355	11	phosphite	phosphite	NOUN
eurjchem-208	355	12	at	at	ADP
eurjchem-208	355	13	80	80	NUM
eurjchem-208	355	14	oc	oc	NOUN
eurjchem-208	355	15	in	in	ADP
eurjchem-208	355	16	the	the	DET
eurjchem-208	355	17	presence	presence	NOUN
eurjchem-208	355	18	of	of	ADP
eurjchem-208	355	19	bf3.et2o	bf3.et2o	PROPN
eurjchem-208	355	20	for	for	ADP
eurjchem-208	355	21	10	10	NUM
eurjchem-208	355	22	hours	hour	NOUN
eurjchem-208	355	23	,	,	PUNCT
eurjchem-208	355	24	afforded	afford	VERB
eurjchem-208	355	25	an	an	DET
eurjchem-208	355	26	interesting	interesting	ADJ
eurjchem-208	355	27	type	type	NOUN
eurjchem-208	355	28	of	of	ADP
eurjchem-208	355	29	phosphorus	phosphorus	NOUN
eurjchem-208	355	30	heterocycle	heterocycle	NOUN
eurjchem-208	355	31	,	,	PUNCT
eurjchem-208	355	32	namely	namely	ADV
eurjchem-208	355	33	bis{3‐(4`‐biphenyl)‐4‐[2‐ethoxy‐6‐phenylamino‐2‐oxo‐	bis{3‐(4`‐biphenyl)‐4‐[2‐ethoxy‐6‐phenylamino‐2‐oxo‐	NOUN
eurjchem-208	355	34	3,4‐dihydro‐2h‐1,4,5,2‐thiadiazaphosphinin‐3‐yl]‐1h‐pyrazol‐	3,4‐dihydro‐2h‐1,4,5,2‐thiadiazaphosphinin‐3‐yl]‐1h‐pyrazol‐	NUM
eurjchem-208	355	35	1‐yl}phosphine	1‐yl}phosphine	NUM
eurjchem-208	355	36	oxide	oxide	NOUN
eurjchem-208	355	37	(	(	PUNCT
eurjchem-208	355	38	22	22	NUM
eurjchem-208	355	39	)	)	PUNCT
eurjchem-208	355	40	(	(	PUNCT
eurjchem-208	355	41	scheme	scheme	NOUN
eurjchem-208	355	42	15	15	NUM
eurjchem-208	355	43	)	)	PUNCT
eurjchem-208	355	44	.	.	PUNCT
eurjchem-208	356	1	the	the	DET
eurjchem-208	356	2	proposed	propose	VERB
eurjchem-208	356	3	mechanism	mechanism	NOUN
eurjchem-208	356	4	for	for	ADP
eurjchem-208	356	5	formation	formation	NOUN
eurjchem-208	356	6	of	of	ADP
eurjchem-208	356	7	22	22	NUM
eurjchem-208	356	8	may	may	AUX
eurjchem-208	356	9	occur	occur	VERB
eurjchem-208	356	10	via	via	ADP
eurjchem-208	356	11	addition	addition	NOUN
eurjchem-208	356	12	of	of	ADP
eurjchem-208	356	13	phosphorus	phosphorus	NOUN
eurjchem-208	356	14	atom	atom	NOUN
eurjchem-208	356	15	of	of	ADP
eurjchem-208	356	16	diethyl	diethyl	NOUN
eurjchem-208	356	17	phosphite	phosphite	NOUN
eurjchem-208	356	18	to	to	ADP
eurjchem-208	356	19	ch	ch	NOUN
eurjchem-208	356	20	=	=	NOUN
eurjchem-208	356	21	nexocyclic	nexocyclic	ADJ
eurjchem-208	356	22	groups	group	NOUN
eurjchem-208	356	23	to	to	PART
eurjchem-208	356	24	give	give	VERB
eurjchem-208	356	25	the	the	DET
eurjchem-208	356	26	nonisolable	nonisolable	ADJ
eurjchem-208	356	27	intermediate	intermediate	ADJ
eurjchem-208	356	28	21	21	NUM
eurjchem-208	356	29	,	,	PUNCT
eurjchem-208	356	30	which	which	DET
eurjchem-208	356	31	underwent	undergo	VERB
eurjchem-208	356	32	cyclization	cyclization	NOUN
eurjchem-208	356	33	by	by	ADP
eurjchem-208	356	34	nucleophilic	nucleophilic	ADJ
eurjchem-208	356	35	attack	attack	NOUN
eurjchem-208	356	36	of	of	ADP
eurjchem-208	356	37	sh	sh	PROPN
eurjchem-208	356	38	groups	group	NOUN
eurjchem-208	356	39	at	at	ADP
eurjchem-208	356	40	phosphonate	phosphonate	ADJ
eurjchem-208	356	41	groups	group	NOUN
eurjchem-208	356	42	to	to	PART
eurjchem-208	356	43	eliminate	eliminate	VERB
eurjchem-208	356	44	two	two	NUM
eurjchem-208	356	45	molecules	molecule	NOUN
eurjchem-208	356	46	of	of	ADP
eurjchem-208	356	47	ethanol	ethanol	NOUN
eurjchem-208	356	48	(	(	PUNCT
eurjchem-208	356	49	scheme	scheme	NOUN
eurjchem-208	356	50	15	15	NUM
eurjchem-208	356	51	)	)	PUNCT
eurjchem-208	356	52	.	.	PUNCT
eurjchem-208	357	1	the	the	DET
eurjchem-208	357	2	ir	ir	PROPN
eurjchem-208	357	3	spectrum	spectrum	NOUN
eurjchem-208	357	4	of	of	ADP
eurjchem-208	357	5	22	22	NUM
eurjchem-208	357	6	displayed	display	VERB
eurjchem-208	357	7	characteristic	characteristic	ADJ
eurjchem-208	357	8	absorption	absorption	NOUN
eurjchem-208	357	9	bands	band	NOUN
eurjchem-208	357	10	for	for	ADP
eurjchem-208	357	11	nh	nh	PROPN
eurjchem-208	357	12	and	and	CCONJ
eurjchem-208	357	13	p	p	X
eurjchem-208	357	14	=	=	ADJ
eurjchem-208	357	15	o	o	NOUN
eurjchem-208	357	16	groups	group	NOUN
eurjchem-208	357	17	at	at	ADP
eurjchem-208	357	18	3404–3276	3404–3276	NUM
eurjchem-208	357	19	and	and	CCONJ
eurjchem-208	357	20	1248–1228	1248–1228	PROPN
eurjchem-208	357	21	cm‐1	cm‐1	PROPN
eurjchem-208	357	22	,	,	PUNCT
eurjchem-208	357	23	respectively	respectively	ADV
eurjchem-208	357	24	.	.	PUNCT
eurjchem-208	358	1	also	also	ADV
eurjchem-208	358	2	,	,	PUNCT
eurjchem-208	358	3	its	its	PRON
eurjchem-208	358	4	1h	1h	NUM
eurjchem-208	358	5	nmr	nmr	NOUN
eurjchem-208	358	6	spectrum	spectrum	NOUN
eurjchem-208	358	7	clearly	clearly	ADV
eurjchem-208	358	8	indicated	indicate	VERB
eurjchem-208	358	9	the	the	DET
eurjchem-208	358	10	presence	presence	NOUN
eurjchem-208	358	11	of	of	ADP
eurjchem-208	358	12	one	one	NUM
eurjchem-208	358	13	ethyl	ethyl	PROPN
eurjchem-208	358	14	ester	ester	NOUN
eurjchem-208	358	15	group	group	NOUN
eurjchem-208	358	16	at	at	ADP
eurjchem-208	358	17	each	each	DET
eurjchem-208	358	18	1,4,5,2‐thiadiaza‐	1,4,5,2‐thiadiaza‐	NOUN
eurjchem-208	358	19	phosphinine	phosphinine	NOUN
eurjchem-208	358	20	moiety	moiety	NOUN
eurjchem-208	358	21	as	as	ADP
eurjchem-208	358	22	a	a	DET
eurjchem-208	358	23	triplet	triplet	NOUN
eurjchem-208	358	24	and	and	CCONJ
eurjchem-208	358	25	quartet	quartet	NOUN
eurjchem-208	358	26	signals	signal	NOUN
eurjchem-208	358	27	at	at	ADP
eurjchem-208	358	28			NUM
eurjchem-208	358	29	1.16	1.16	NUM
eurjchem-208	358	30	and	and	CCONJ
eurjchem-208	358	31	3.96	3.96	NUM
eurjchem-208	358	32	ppm	ppm	NOUN
eurjchem-208	358	33	(	(	PUNCT
eurjchem-208	358	34	j=	j=	ADP
eurjchem-208	358	35	8.2	8.2	NUM
eurjchem-208	358	36	hz	hz	NOUN
eurjchem-208	358	37	)	)	PUNCT
eurjchem-208	358	38	,	,	PUNCT
eurjchem-208	358	39	respectively	respectively	ADV
eurjchem-208	358	40	,	,	PUNCT
eurjchem-208	358	41	in	in	ADP
eurjchem-208	358	42	addition	addition	NOUN
eurjchem-208	358	43	to	to	ADP
eurjchem-208	358	44	one	one	NUM
eurjchem-208	358	45	doublet	doublet	NOUN
eurjchem-208	358	46	and	and	CCONJ
eurjchem-208	358	47	two	two	NUM
eurjchem-208	358	48	singlet	singlet	ADJ
eurjchem-208	358	49	signals	signal	NOUN
eurjchem-208	358	50	at	at	ADP
eurjchem-208	358	51			NUM
eurjchem-208	358	52	4.90	4.90	NUM
eurjchem-208	358	53	(	(	PUNCT
eurjchem-208	358	54	jph=	jph=	PROPN
eurjchem-208	358	55	20.4	20.4	NUM
eurjchem-208	358	56	hz	hz	NOUN
eurjchem-208	358	57	)	)	PUNCT
eurjchem-208	358	58	,	,	PUNCT
eurjchem-208	358	59	9.83	9.83	NUM
eurjchem-208	358	60	and	and	CCONJ
eurjchem-208	358	61	11.69	11.69	NUM
eurjchem-208	358	62	ppm	ppm	NOUN
eurjchem-208	358	63	assigned	assign	VERB
eurjchem-208	358	64	to	to	ADP
eurjchem-208	358	65	ch	ch	NOUN
eurjchem-208	358	66	–	–	PUNCT
eurjchem-208	358	67	p	p	NOUN
eurjchem-208	358	68	and	and	CCONJ
eurjchem-208	358	69	each	each	DET
eurjchem-208	358	70	two	two	NUM
eurjchem-208	358	71	nhprotons	nhproton	NOUN
eurjchem-208	358	72	,	,	PUNCT
eurjchem-208	358	73	respectively	respectively	ADV
eurjchem-208	358	74	.	.	PUNCT
eurjchem-208	359	1	moreover	moreover	ADV
eurjchem-208	359	2	,	,	PUNCT
eurjchem-208	359	3	its	its	PRON
eurjchem-208	359	4	31p	31p	NUM
eurjchem-208	359	5	nmr	nmr	NOUN
eurjchem-208	359	6	spectrum	spectrum	NOUN
eurjchem-208	359	7	exhibited	exhibit	VERB
eurjchem-208	359	8	two	two	NUM
eurjchem-208	359	9	signals	signal	NOUN
eurjchem-208	359	10	at	at	ADP
eurjchem-208	359	11			NUM
eurjchem-208	359	12	6.62	6.62	NUM
eurjchem-208	359	13	and	and	CCONJ
eurjchem-208	359	14	28.08	28.08	NUM
eurjchem-208	359	15	ppm	ppm	NOUN
eurjchem-208	359	16	corresponding	correspond	VERB
eurjchem-208	359	17	to	to	ADP
eurjchem-208	359	18	h	h	NUM
eurjchem-208	359	19	–	–	PUNCT
eurjchem-208	359	20	p	p	X
eurjchem-208	359	21	=	=	X
eurjchem-208	359	22	o	o	X
eurjchem-208	359	23	and	and	CCONJ
eurjchem-208	359	24	eto	eto	PROPN
eurjchem-208	359	25	–	–	PUNCT
eurjchem-208	359	26	p	p	X
eurjchem-208	359	27	=	=	ADJ
eurjchem-208	359	28	o	o	NOUN
eurjchem-208	359	29	groups	group	NOUN
eurjchem-208	359	30	,	,	PUNCT
eurjchem-208	359	31	respectively	respectively	ADV
eurjchem-208	359	32	[	[	X
eurjchem-208	359	33	15	15	NUM
eurjchem-208	359	34	]	]	SYM
eurjchem-208	359	35	.	.	PUNCT
eurjchem-208	360	1	3.2	3.2	NUM
eurjchem-208	360	2	.	.	PUNCT
eurjchem-208	361	1	in	in	ADP
eurjchem-208	361	2	vitro	vitro	X
eurjchem-208	361	3	antimicrobial	antimicrobial	ADJ
eurjchem-208	361	4	activity	activity	NOUN
eurjchem-208	361	5	all	all	DET
eurjchem-208	361	6	the	the	DET
eurjchem-208	361	7	synthesized	synthesize	VERB
eurjchem-208	361	8	compounds	compound	NOUN
eurjchem-208	361	9	were	be	AUX
eurjchem-208	361	10	evaluated	evaluate	VERB
eurjchem-208	361	11	in	in	ADP
eurjchem-208	361	12	vitro	vitro	X
eurjchem-208	361	13	for	for	ADP
eurjchem-208	361	14	their	their	PRON
eurjchem-208	361	15	antibacterial	antibacterial	ADJ
eurjchem-208	361	16	activity	activity	NOUN
eurjchem-208	361	17	against	against	ADP
eurjchem-208	361	18	staphylococcus	staphylococcus	NOUN
eurjchem-208	361	19	aureus	aureus	NOUN
eurjchem-208	361	20	(	(	PUNCT
eurjchem-208	361	21	atcc	atcc	NOUN
eurjchem-208	361	22	25923	25923	NUM
eurjchem-208	361	23	)	)	PUNCT
eurjchem-208	361	24	and	and	CCONJ
eurjchem-208	361	25	streptococcus	streptococcus	VERB
eurjchem-208	361	26	pyogenes	pyogene	NOUN
eurjchem-208	361	27	(	(	PUNCT
eurjchem-208	361	28	atcc	atcc	NOUN
eurjchem-208	361	29	19615	19615	NUM
eurjchem-208	361	30	)	)	PUNCT
eurjchem-208	361	31	as	as	ADP
eurjchem-208	361	32	examples	example	NOUN
eurjchem-208	361	33	of	of	ADP
eurjchem-208	361	34	gram	gram	NOUN
eurjchem-208	361	35	positive	positive	ADJ
eurjchem-208	361	36	bacteria	bacteria	NOUN
eurjchem-208	361	37	and	and	CCONJ
eurjchem-208	361	38	pseudomonas	pseudomona	NOUN
eurjchem-208	361	39	fluorescens	fluorescen	NOUN
eurjchem-208	361	40	(	(	PUNCT
eurjchem-208	361	41	s	s	NOUN
eurjchem-208	361	42	97	97	NUM
eurjchem-208	361	43	)	)	PUNCT
eurjchem-208	361	44	and	and	CCONJ
eurjchem-208	361	45	pseudomonas	pseudomona	NOUN
eurjchem-208	361	46	phaseolicola	phaseolicola	PROPN
eurjchem-208	361	47	(	(	PUNCT
eurjchem-208	361	48	gspb	gspb	NOUN
eurjchem-208	361	49	2828	2828	NUM
eurjchem-208	361	50	)	)	PUNCT
eurjchem-208	361	51	as	as	ADP
eurjchem-208	361	52	examples	example	NOUN
eurjchem-208	361	53	of	of	ADP
eurjchem-208	361	54	gram	gram	NOUN
eurjchem-208	361	55	negative	negative	ADJ
eurjchem-208	361	56	bacteria	bacteria	NOUN
eurjchem-208	361	57	.	.	PUNCT
eurjchem-208	362	1	they	they	PRON
eurjchem-208	362	2	were	be	AUX
eurjchem-208	362	3	also	also	ADV
eurjchem-208	362	4	evaluated	evaluate	VERB
eurjchem-208	362	5	in	in	ADP
eurjchem-208	362	6	vitro	vitro	X
eurjchem-208	362	7	for	for	ADP
eurjchem-208	362	8	their	their	PRON
eurjchem-208	362	9	antifungal	antifungal	ADJ
eurjchem-208	362	10	activity	activity	NOUN
eurjchem-208	362	11	against	against	ADP
eurjchem-208	362	12	fusariumoxysporum	fusariumoxysporum	NOUN
eurjchem-208	362	13	and	and	CCONJ
eurjchem-208	362	14	aspergillusfumigatus	aspergillusfumigatus	NOUN
eurjchem-208	362	15	fungal	fungal	ADJ
eurjchem-208	362	16	strains	strain	NOUN
eurjchem-208	362	17	.	.	PUNCT
eurjchem-208	363	1	agar‐diffusion	agar‐diffusion	NOUN
eurjchem-208	363	2	technique	technique	NOUN
eurjchem-208	363	3	was	be	AUX
eurjchem-208	363	4	used	use	VERB
eurjchem-208	363	5	for	for	ADP
eurjchem-208	363	6	the	the	DET
eurjchem-208	363	7	determination	determination	NOUN
eurjchem-208	363	8	of	of	ADP
eurjchem-208	363	9	the	the	DET
eurjchem-208	363	10	preliminary	preliminary	ADJ
eurjchem-208	363	11	antibacterial	antibacterial	ADJ
eurjchem-208	363	12	and	and	CCONJ
eurjchem-208	363	13	antifungal	antifungal	ADJ
eurjchem-208	363	14	activity	activity	NOUN
eurjchem-208	363	15	[	[	X
eurjchem-208	363	16	50	50	NUM
eurjchem-208	363	17	]	]	PUNCT
eurjchem-208	363	18	.	.	PUNCT
eurjchem-208	364	1	the	the	DET
eurjchem-208	364	2	test	test	NOUN
eurjchem-208	364	3	was	be	AUX
eurjchem-208	364	4	performed	perform	VERB
eurjchem-208	364	5	on	on	ADP
eurjchem-208	364	6	medium	medium	ADJ
eurjchem-208	364	7	potato	potato	NOUN
eurjchem-208	364	8	dextrose	dextrose	NOUN
eurjchem-208	364	9	agars	agar	NOUN
eurjchem-208	364	10	(	(	PUNCT
eurjchem-208	364	11	pda	pda	NOUN
eurjchem-208	364	12	)	)	PUNCT
eurjchem-208	364	13	which	which	PRON
eurjchem-208	364	14	contain	contain	VERB
eurjchem-208	364	15	infusion	infusion	NOUN
eurjchem-208	364	16	of	of	ADP
eurjchem-208	364	17	200	200	NUM
eurjchem-208	364	18	g	g	NOUN
eurjchem-208	364	19	potatoes	potato	NOUN
eurjchem-208	364	20	,	,	PUNCT
eurjchem-208	364	21	6	6	NUM
eurjchem-208	364	22	g	g	NOUN
eurjchem-208	364	23	dextrose	dextrose	NOUN
eurjchem-208	364	24	and	and	CCONJ
eurjchem-208	364	25	15	15	NUM
eurjchem-208	364	26	g	g	NOUN
eurjchem-208	364	27	agar	agar	NOUN
eurjchem-208	364	28	[	[	X
eurjchem-208	364	29	51	51	NUM
eurjchem-208	364	30	]	]	PUNCT
eurjchem-208	364	31	.	.	PUNCT
eurjchem-208	365	1	uniform	uniform	ADJ
eurjchem-208	365	2	size	size	NOUN
eurjchem-208	365	3	filter	filter	NOUN
eurjchem-208	365	4	paper	paper	NOUN
eurjchem-208	365	5	disks	disk	NOUN
eurjchem-208	365	6	(	(	PUNCT
eurjchem-208	365	7	3	3	NUM
eurjchem-208	365	8	disks	disk	NOUN
eurjchem-208	365	9	per	per	ADP
eurjchem-208	365	10	compound	compound	NOUN
eurjchem-208	365	11	)	)	PUNCT
eurjchem-208	365	12	were	be	AUX
eurjchem-208	365	13	impregnated	impregnate	VERB
eurjchem-208	365	14	by	by	ADP
eurjchem-208	365	15	equal	equal	ADJ
eurjchem-208	365	16	volume	volume	NOUN
eurjchem-208	365	17	(	(	PUNCT
eurjchem-208	365	18	10	10	NUM
eurjchem-208	365	19	µl	µl	NOUN
eurjchem-208	365	20	)	)	PUNCT
eurjchem-208	365	21	from	from	ADP
eurjchem-208	365	22	the	the	DET
eurjchem-208	365	23	concentrations	concentration	NOUN
eurjchem-208	365	24	of	of	ADP
eurjchem-208	365	25	1	1	NUM
eurjchem-208	365	26	and	and	CCONJ
eurjchem-208	365	27	2	2	NUM
eurjchem-208	365	28	mg	mg	PROPN
eurjchem-208	365	29	/	/	SYM
eurjchem-208	365	30	cm3	cm3	NOUN
eurjchem-208	365	31	dissolved	dissolve	VERB
eurjchem-208	365	32	compounds	compound	NOUN
eurjchem-208	365	33	in	in	ADP
eurjchem-208	365	34	dimethylformamide	dimethylformamide	NOUN
eurjchem-208	365	35	(	(	PUNCT
eurjchem-208	365	36	dmf	dmf	PROPN
eurjchem-208	365	37	)	)	PUNCT
eurjchem-208	365	38	and	and	CCONJ
eurjchem-208	365	39	carefully	carefully	ADV
eurjchem-208	365	40	placed	place	VERB
eurjchem-208	365	41	on	on	ADP
eurjchem-208	365	42	inoculated	inoculate	VERB
eurjchem-208	365	43	agar	agar	NOUN
eurjchem-208	365	44	surface	surface	NOUN
eurjchem-208	365	45	.	.	PUNCT
eurjchem-208	366	1	after	after	ADP
eurjchem-208	366	2	incubation	incubation	NOUN
eurjchem-208	366	3	for	for	ADP
eurjchem-208	366	4	36	36	NUM
eurjchem-208	366	5	h	h	NOUN
eurjchem-208	366	6	at	at	ADP
eurjchem-208	366	7	27	27	NUM
eurjchem-208	366	8	°	°	NOUN
eurjchem-208	366	9	c	c	NOUN
eurjchem-208	366	10	in	in	ADP
eurjchem-208	366	11	the	the	DET
eurjchem-208	366	12	case	case	NOUN
eurjchem-208	366	13	of	of	ADP
eurjchem-208	366	14	bacteria	bacteria	NOUN
eurjchem-208	366	15	and	and	CCONJ
eurjchem-208	366	16	for	for	ADP
eurjchem-208	366	17	48	48	NUM
eurjchem-208	366	18	h	h	NOUN
eurjchem-208	366	19	at	at	ADP
eurjchem-208	366	20	24	24	NUM
eurjchem-208	366	21	°	°	NOUN
eurjchem-208	366	22	c	c	NOUN
eurjchem-208	366	23	in	in	ADP
eurjchem-208	366	24	the	the	DET
eurjchem-208	366	25	case	case	NOUN
eurjchem-208	366	26	of	of	ADP
eurjchem-208	366	27	fungi	fungi	PROPN
eurjchem-208	366	28	.	.	PUNCT
eurjchem-208	367	1	cephalothin	cephalothin	PROPN
eurjchem-208	367	2	,	,	PUNCT
eurjchem-208	367	3	chloramphenicol	chloramphenicol	NOUN
eurjchem-208	367	4	and	and	CCONJ
eurjchem-208	367	5	cycloheximide	cycloheximide	NOUN
eurjchem-208	367	6	were	be	AUX
eurjchem-208	367	7	used	use	VERB
eurjchem-208	367	8	as	as	ADP
eurjchem-208	367	9	reference	reference	NOUN
eurjchem-208	367	10	drugs	drug	NOUN
eurjchem-208	367	11	at	at	ADP
eurjchem-208	367	12	30	30	NUM
eurjchem-208	367	13	µg	µg	NOUN
eurjchem-208	367	14	/	/	SYM
eurjchem-208	367	15	cm3	cm3	NOUN
eurjchem-208	367	16	for	for	ADP
eurjchem-208	367	17	gram	gram	NOUN
eurjchem-208	367	18	positive	positive	ADJ
eurjchem-208	367	19	bacteria	bacteria	NOUN
eurjchem-208	367	20	,	,	PUNCT
eurjchem-208	367	21	gram	gram	NOUN
eurjchem-208	367	22	negative	negative	ADJ
eurjchem-208	367	23	bacteria	bacteria	NOUN
eurjchem-208	367	24	and	and	CCONJ
eurjchem-208	367	25	fungi	fungus	NOUN
eurjchem-208	367	26	,	,	PUNCT
eurjchem-208	367	27	respectively	respectively	ADV
eurjchem-208	367	28	.	.	PUNCT
eurjchem-208	368	1	the	the	DET
eurjchem-208	368	2	results	result	NOUN
eurjchem-208	368	3	were	be	AUX
eurjchem-208	368	4	recorded	record	VERB
eurjchem-208	368	5	for	for	ADP
eurjchem-208	368	6	each	each	DET
eurjchem-208	368	7	tested	test	VERB
eurjchem-208	368	8	abdel‐aziz	abdel‐aziz	PROPN
eurjchem-208	368	9	et	et	NOUN
eurjchem-208	368	10	al./	al./	ADV
eurjchem-208	368	11	european	european	PROPN
eurjchem-208	368	12	journal	journal	PROPN
eurjchem-208	368	13	of	of	ADP
eurjchem-208	368	14	chemistry	chemistry	NOUN
eurjchem-208	368	15	2	2	NUM
eurjchem-208	368	16	(	(	PUNCT
eurjchem-208	368	17	1	1	NUM
eurjchem-208	368	18	)	)	PUNCT
eurjchem-208	368	19	(	(	PUNCT
eurjchem-208	368	20	2011	2011	NUM
eurjchem-208	368	21	)	)	PUNCT
eurjchem-208	368	22	25‐35	25‐35	NUM
eurjchem-208	368	23	33	33	NUM
eurjchem-208	368	24	compound	compound	NOUN
eurjchem-208	368	25	as	as	ADP
eurjchem-208	368	26	average	average	ADJ
eurjchem-208	368	27	diameter	diameter	NOUN
eurjchem-208	368	28	of	of	ADP
eurjchem-208	368	29	inhibition	inhibition	NOUN
eurjchem-208	368	30	zones	zone	NOUN
eurjchem-208	368	31	of	of	ADP
eurjchem-208	368	32	bacterial	bacterial	ADJ
eurjchem-208	368	33	or	or	CCONJ
eurjchem-208	368	34	fungal	fungal	ADJ
eurjchem-208	368	35	around	around	ADP
eurjchem-208	368	36	the	the	DET
eurjchem-208	368	37	disks	disk	NOUN
eurjchem-208	368	38	in	in	ADP
eurjchem-208	368	39	mm	mm	PROPN
eurjchem-208	368	40	at	at	ADP
eurjchem-208	368	41	the	the	DET
eurjchem-208	368	42	concentrations	concentration	NOUN
eurjchem-208	368	43	1	1	NUM
eurjchem-208	368	44	and	and	CCONJ
eurjchem-208	368	45	2	2	NUM
eurjchem-208	368	46	mg/	mg/	NOUN
eurjchem-208	368	47	cm3	cm3	NOUN
eurjchem-208	368	48	(	(	PUNCT
eurjchem-208	368	49	tables	table	NOUN
eurjchem-208	368	50	1‐3	1‐3	NUM
eurjchem-208	368	51	)	)	PUNCT
eurjchem-208	368	52	.	.	PUNCT
eurjchem-208	369	1	h	h	NOUN
eurjchem-208	369	2	-	-	PUNCT
eurjchem-208	369	3	p(o)(oet)2	p(o)(oet)2	NOUN
eurjchem-208	369	4	n	n	CCONJ
eurjchem-208	369	5	n	n	PROPN
eurjchem-208	369	6	p	p	NOUN
eurjchem-208	369	7	n	n	CCONJ
eurjchem-208	369	8	n	n	PRON
eurjchem-208	369	9	h	h	NOUN
eurjchem-208	369	10	o	o	NOUN
eurjchem-208	369	11	arar	arar	NOUN
eurjchem-208	369	12	n	n	PROPN
eurjchem-208	369	13	h	h	NOUN
eurjchem-208	370	1	n	n	NOUN
eurjchem-208	370	2	s	s	VERB
eurjchem-208	371	1	hn	hn	PROPN
eurjchem-208	371	2	n	n	PROPN
eurjchem-208	371	3	h	h	NOUN
eurjchem-208	372	1	ns	ns	PROPN
eurjchem-208	372	2	nh	nh	PROPN
eurjchem-208	372	3	ph	ph	ADJ
eurjchem-208	372	4	ph	ph	PROPN
eurjchem-208	372	5	n	n	CCONJ
eurjchem-208	372	6	n	n	NOUN
eurjchem-208	372	7	p	p	NOUN
eurjchem-208	372	8	n	n	CCONJ
eurjchem-208	372	9	n	n	PRON
eurjchem-208	372	10	h	h	NOUN
eurjchem-208	372	11	o	o	NOUN
eurjchem-208	372	12	arar	arar	NOUN
eurjchem-208	372	13	n	n	PROPN
eurjchem-208	372	14	h	h	NOUN
eurjchem-208	373	1	n	n	ADV
eurjchem-208	373	2	sh	sh	INTJ
eurjchem-208	374	1	hn	hn	INTJ
eurjchem-208	374	2	n	n	PROPN
eurjchem-208	374	3	h	h	NOUN
eurjchem-208	374	4	nhs	nhs	PROPN
eurjchem-208	374	5	nh	nh	PROPN
eurjchem-208	374	6	ph	ph	PROPN
eurjchem-208	374	7	ph	ph	PROPN
eurjchem-208	374	8	p	p	NOUN
eurjchem-208	374	9	h	h	NOUN
eurjchem-208	375	1	o	o	NOUN
eurjchem-208	375	2	p	p	NOUN
eurjchem-208	376	1	h	h	NOUN
eurjchem-208	376	2	o	o	NOUN
eurjchem-208	376	3	oet	oet	VERB
eurjchem-208	376	4	etooeteto	etooeteto	VERB
eurjchem-208	376	5	n	n	CCONJ
eurjchem-208	376	6	n	n	PROPN
eurjchem-208	376	7	p	p	NOUN
eurjchem-208	376	8	n	n	CCONJ
eurjchem-208	376	9	n	n	PRON
eurjchem-208	376	10	h	h	NOUN
eurjchem-208	376	11	o	o	NOUN
eurjchem-208	376	12	arar	arar	PROPN
eurjchem-208	377	1	n	n	PROPN
eurjchem-208	377	2	h	h	NOUN
eurjchem-208	378	1	n	n	CCONJ
eurjchem-208	379	1	n	n	PROPN
eurjchem-208	380	1	h	h	NOUN
eurjchem-208	381	1	n	n	CCONJ
eurjchem-208	381	2	p	p	NOUN
eurjchem-208	381	3	h	h	NOUN
eurjchem-208	382	1	o	o	NOUN
eurjchem-208	382	2	p	p	NOUN
eurjchem-208	383	1	h	h	NOUN
eurjchem-208	383	2	o	o	NOUN
eurjchem-208	383	3	s	s	NOUN
eurjchem-208	383	4	etooets	etooet	NOUN
eurjchem-208	383	5	h	h	PROPN
eurjchem-208	383	6	nh	nh	PROPN
eurjchem-208	383	7	n	n	CCONJ
eurjchem-208	383	8	ph	ph	NOUN
eurjchem-208	383	9	ph	ph	NOUN
eurjchem-208	383	10	-2	-2	INTJ
eurjchem-208	383	11	etoh	etoh	PROPN
eurjchem-208	383	12	18	18	NUM
eurjchem-208	383	13	21	21	NUM
eurjchem-208	383	14	22	22	NUM
eurjchem-208	383	15	bf3.et2o	bf3.et2o	NOUN
eurjchem-208	383	16	51	51	NUM
eurjchem-208	383	17	%	%	NOUN
eurjchem-208	383	18	scheme	scheme	NOUN
eurjchem-208	383	19	15	15	NUM
eurjchem-208	383	20	table	table	NOUN
eurjchem-208	383	21	1	1	NUM
eurjchem-208	383	22	.	.	PUNCT
eurjchem-208	383	23	antibacterial	antibacterial	ADJ
eurjchem-208	383	24	activity	activity	NOUN
eurjchem-208	383	25	(	(	PUNCT
eurjchem-208	383	26	gram	gram	NOUN
eurjchem-208	383	27	positive	positive	ADJ
eurjchem-208	383	28	bacteria	bacteria	NOUN
eurjchem-208	383	29	)	)	PUNCT
eurjchem-208	383	30	of	of	ADP
eurjchem-208	383	31	the	the	DET
eurjchem-208	383	32	synthesized	synthesize	VERB
eurjchem-208	383	33	compounds	compound	NOUN
eurjchem-208	383	34	3‐22	3‐22	NUM
eurjchem-208	383	35	at	at	ADP
eurjchem-208	383	36	1	1	NUM
eurjchem-208	383	37	and	and	CCONJ
eurjchem-208	383	38	2	2	NUM
eurjchem-208	383	39	mg	mg	NUM
eurjchem-208	383	40	/	/	SYM
eurjchem-208	383	41	cm3	cm3	NOUN
eurjchem-208	383	42	by	by	ADP
eurjchem-208	383	43	disc	disc	NOUN
eurjchem-208	383	44	diffusion	diffusion	NOUN
eurjchem-208	383	45	assay	assay	PROPN
eurjchem-208	383	46	*	*	PROPN
eurjchem-208	383	47	.	.	PUNCT
eurjchem-208	384	1	compound	compound	NOUN
eurjchem-208	384	2	diameter	diameter	NOUN
eurjchem-208	384	3	of	of	ADP
eurjchem-208	384	4	zone	zone	NOUN
eurjchem-208	384	5	of	of	ADP
eurjchem-208	384	6	inhibition	inhibition	NOUN
eurjchem-208	384	7	in	in	ADP
eurjchem-208	384	8	mm	mm	PROPN
eurjchem-208	384	9	gram‐positive	gram‐positive	ADJ
eurjchem-208	384	10	bacteria	bacteria	NOUN
eurjchem-208	384	11	s.	s.	PROPN
eurjchem-208	384	12	aureus	aureus	PROPN
eurjchem-208	384	13	(	(	PUNCT
eurjchem-208	384	14	atcc	atcc	PROPN
eurjchem-208	384	15	25923	25923	NUM
eurjchem-208	384	16	)	)	PUNCT
eurjchem-208	385	1	s.	s.	PROPN
eurjchem-208	385	2	pyogenes	pyogenes	PROPN
eurjchem-208	385	3	(	(	PUNCT
eurjchem-208	385	4	atcc	atcc	NOUN
eurjchem-208	385	5	19615	19615	NUM
eurjchem-208	385	6	)	)	PUNCT
eurjchem-208	385	7	2	2	NUM
eurjchem-208	385	8	mg	mg	PROPN
eurjchem-208	385	9	/	/	SYM
eurjchem-208	385	10	cm3	cm3	NOUN
eurjchem-208	385	11	1	1	NUM
eurjchem-208	385	12	mg	mg	NOUN
eurjchem-208	385	13	/	/	SYM
eurjchem-208	385	14	cm3	cm3	NOUN
eurjchem-208	385	15	2	2	NUM
eurjchem-208	385	16	mg	mg	PROPN
eurjchem-208	385	17	/	/	SYM
eurjchem-208	385	18	cm3	cm3	NOUN
eurjchem-208	385	19	1	1	NUM
eurjchem-208	385	20	mg	mg	NUM
eurjchem-208	385	21	/	/	SYM
eurjchem-208	385	22	cm3	cm3	PROPN
eurjchem-208	385	23	3a	3a	NUM
eurjchem-208	385	24	−	−	ADP
eurjchem-208	385	25	−	−	PROPN
eurjchem-208	385	26	−	−	PROPN
eurjchem-208	385	27	−	−	PROPN
eurjchem-208	385	28	3b	3b	NOUN
eurjchem-208	385	29	−	−	NOUN
eurjchem-208	385	30	−	−	NOUN
eurjchem-208	385	31	−	−	PROPN
eurjchem-208	385	32	−	−	PROPN
eurjchem-208	385	33	3c	3c	NUM
eurjchem-208	385	34	−	−	NOUN
eurjchem-208	385	35	−	−	PROPN
eurjchem-208	385	36	−	−	PROPN
eurjchem-208	385	37	−	−	PROPN
eurjchem-208	385	38	3d	3d	NOUN
eurjchem-208	385	39	−	−	PROPN
eurjchem-208	385	40	−	−	PROPN
eurjchem-208	385	41	−	−	PROPN
eurjchem-208	385	42	−	−	PROPN
eurjchem-208	385	43	4a	4a	NOUN
eurjchem-208	385	44	10	10	NUM
eurjchem-208	385	45	8	8	NUM
eurjchem-208	385	46	7	7	NUM
eurjchem-208	385	47	−	−	PROPN
eurjchem-208	385	48	4b	4b	NOUN
eurjchem-208	385	49	10	10	NUM
eurjchem-208	385	50	8	8	NUM
eurjchem-208	385	51	8	8	NUM
eurjchem-208	385	52	5	5	NUM
eurjchem-208	385	53	6	6	NUM
eurjchem-208	385	54	10	10	NUM
eurjchem-208	385	55	8	8	NUM
eurjchem-208	385	56	7	7	NUM
eurjchem-208	385	57	6	6	NUM
eurjchem-208	385	58	8	8	NUM
eurjchem-208	385	59	10	10	NUM
eurjchem-208	385	60	7	7	NUM
eurjchem-208	385	61	8	8	NUM
eurjchem-208	385	62	5	5	NUM
eurjchem-208	385	63	9	9	NUM
eurjchem-208	385	64	8	8	NUM
eurjchem-208	385	65	5	5	NUM
eurjchem-208	385	66	5	5	NUM
eurjchem-208	385	67	−	−	NUM
eurjchem-208	385	68	10	10	NUM
eurjchem-208	385	69	14	14	NUM
eurjchem-208	385	70	8	8	NUM
eurjchem-208	385	71	18	18	NUM
eurjchem-208	385	72	14	14	NUM
eurjchem-208	385	73	11	11	NUM
eurjchem-208	385	74	21	21	NUM
eurjchem-208	385	75	12	12	NUM
eurjchem-208	385	76	17	17	NUM
eurjchem-208	385	77	14	14	NUM
eurjchem-208	385	78	12	12	NUM
eurjchem-208	385	79	8	8	NUM
eurjchem-208	385	80	6	6	NUM
eurjchem-208	385	81	7	7	NUM
eurjchem-208	385	82	−	−	NUM
eurjchem-208	385	83	14	14	NUM
eurjchem-208	385	84	10	10	NUM
eurjchem-208	385	85	7	7	NUM
eurjchem-208	385	86	11	11	NUM
eurjchem-208	385	87	9	9	NUM
eurjchem-208	385	88	16	16	NUM
eurjchem-208	385	89	24	24	NUM
eurjchem-208	385	90	17	17	NUM
eurjchem-208	385	91	19	19	NUM
eurjchem-208	385	92	13	13	NUM
eurjchem-208	385	93	18	18	NUM
eurjchem-208	385	94	11	11	NUM
eurjchem-208	385	95	7	7	NUM
eurjchem-208	385	96	8	8	NUM
eurjchem-208	385	97	5	5	NUM
eurjchem-208	385	98	20	20	NUM
eurjchem-208	385	99	16	16	NUM
eurjchem-208	385	100	11	11	NUM
eurjchem-208	385	101	20	20	NUM
eurjchem-208	385	102	15	15	NUM
eurjchem-208	385	103	22	22	NUM
eurjchem-208	385	104	30	30	NUM
eurjchem-208	385	105	24	24	NUM
eurjchem-208	385	106	26	26	NUM
eurjchem-208	385	107	20	20	NUM
eurjchem-208	385	108	cephalothin	cephalothin	NUM
eurjchem-208	385	109	28	28	NUM
eurjchem-208	385	110	30	30	NUM
eurjchem-208	385	111	*	*	ADP
eurjchem-208	385	112	less	less	ADV
eurjchem-208	385	113	active	active	ADJ
eurjchem-208	385	114	:	:	PUNCT
eurjchem-208	385	115	6‐12	6‐12	NUM
eurjchem-208	385	116	mm	mm	INTJ
eurjchem-208	385	117	;	;	PUNCT
eurjchem-208	385	118	moderately	moderately	ADV
eurjchem-208	385	119	active	active	ADJ
eurjchem-208	385	120	:	:	PUNCT
eurjchem-208	385	121	13‐19	13‐19	NUM
eurjchem-208	385	122	mm	mm	NOUN
eurjchem-208	385	123	;	;	PUNCT
eurjchem-208	385	124	highly	highly	ADV
eurjchem-208	385	125	active	active	ADJ
eurjchem-208	385	126	:	:	PUNCT
eurjchem-208	385	127	20‐30	20‐30	PROPN
eurjchem-208	385	128	mm	mm	INTJ
eurjchem-208	385	129	;	;	PUNCT
eurjchem-208	385	130	–	–	PUNCT
eurjchem-208	385	131	:	:	PUNCT
eurjchem-208	385	132	no	no	DET
eurjchem-208	385	133	inhibition	inhibition	NOUN
eurjchem-208	385	134	or	or	CCONJ
eurjchem-208	385	135	inhibition	inhibition	NOUN
eurjchem-208	385	136	less	less	ADJ
eurjchem-208	385	137	than	than	ADP
eurjchem-208	385	138	5	5	NUM
eurjchem-208	385	139	mm	mm	NOUN
eurjchem-208	385	140	.	.	PROPN
eurjchem-208	385	141	1	1	NUM
eurjchem-208	385	142	)	)	PUNCT
eurjchem-208	385	143	the	the	DET
eurjchem-208	385	144	investigation	investigation	NOUN
eurjchem-208	385	145	of	of	ADP
eurjchem-208	385	146	antibacterial	antibacterial	ADJ
eurjchem-208	385	147	and	and	CCONJ
eurjchem-208	385	148	antifungal	antifungal	ADJ
eurjchem-208	385	149	screening	screen	VERB
eurjchem-208	385	150	data	datum	NOUN
eurjchem-208	385	151	in	in	ADP
eurjchem-208	385	152	tables	table	NOUN
eurjchem-208	385	153	1‐3	1‐3	PROPN
eurjchem-208	385	154	revealed	reveal	VERB
eurjchem-208	385	155	that	that	SCONJ
eurjchem-208	385	156	most	most	ADJ
eurjchem-208	385	157	of	of	ADP
eurjchem-208	385	158	the	the	DET
eurjchem-208	385	159	synthesized	synthesize	VERB
eurjchem-208	385	160	compounds	compound	NOUN
eurjchem-208	385	161	were	be	AUX
eurjchem-208	385	162	found	find	VERB
eurjchem-208	385	163	to	to	PART
eurjchem-208	385	164	possess	possess	VERB
eurjchem-208	385	165	various	various	ADJ
eurjchem-208	385	166	antimicrobial	antimicrobial	ADJ
eurjchem-208	385	167	activities	activity	NOUN
eurjchem-208	385	168	towards	towards	ADP
eurjchem-208	385	169	all	all	DET
eurjchem-208	385	170	the	the	DET
eurjchem-208	385	171	microorganisms	microorganism	NOUN
eurjchem-208	385	172	.	.	PUNCT
eurjchem-208	386	1	2	2	NUM
eurjchem-208	386	2	)	)	PUNCT
eurjchem-208	386	3	in	in	ADP
eurjchem-208	386	4	general	general	ADJ
eurjchem-208	386	5	,	,	PUNCT
eurjchem-208	386	6	most	most	ADJ
eurjchem-208	386	7	of	of	ADP
eurjchem-208	386	8	the	the	DET
eurjchem-208	386	9	synthesized	synthesize	VERB
eurjchem-208	386	10	compounds	compound	NOUN
eurjchem-208	386	11	exhibited	exhibit	VERB
eurjchem-208	386	12	antibacterial	antibacterial	ADJ
eurjchem-208	386	13	activity	activity	NOUN
eurjchem-208	386	14	better	well	ADJ
eurjchem-208	386	15	than	than	ADP
eurjchem-208	386	16	antifungal	antifungal	ADJ
eurjchem-208	386	17	activity	activity	NOUN
eurjchem-208	386	18	.	.	PUNCT
eurjchem-208	387	1	3	3	X
eurjchem-208	387	2	)	)	PUNCT
eurjchem-208	387	3	most	most	ADJ
eurjchem-208	387	4	of	of	ADP
eurjchem-208	387	5	the	the	DET
eurjchem-208	387	6	synthesized	synthesize	VERB
eurjchem-208	387	7	compounds	compound	NOUN
eurjchem-208	387	8	showed	show	VERB
eurjchem-208	387	9	inhibitions	inhibition	NOUN
eurjchem-208	387	10	against	against	ADP
eurjchem-208	387	11	gram‐positive	gram‐positive	ADJ
eurjchem-208	387	12	bacteria	bacteria	NOUN
eurjchem-208	387	13	more	more	ADJ
eurjchem-208	387	14	than	than	ADP
eurjchem-208	387	15	gram‐negative	gram‐negative	ADJ
eurjchem-208	387	16	bacteria	bacteria	NOUN
eurjchem-208	387	17	except	except	SCONJ
eurjchem-208	387	18	12	12	NUM
eurjchem-208	387	19	which	which	PRON
eurjchem-208	387	20	showed	show	VERB
eurjchem-208	387	21	also	also	ADV
eurjchem-208	387	22	high	high	ADJ
eurjchem-208	387	23	activity	activity	NOUN
eurjchem-208	387	24	against	against	ADP
eurjchem-208	387	25	p.	p.	PROPN
eurjchem-208	387	26	phaseolicola	phaseolicola	PROPN
eurjchem-208	387	27	.	.	PUNCT
eurjchem-208	388	1	4	4	NUM
eurjchem-208	388	2	)	)	PUNCT
eurjchem-208	388	3	most	most	ADJ
eurjchem-208	388	4	of	of	ADP
eurjchem-208	388	5	the	the	DET
eurjchem-208	388	6	synthesized	synthesize	VERB
eurjchem-208	388	7	compounds	compound	NOUN
eurjchem-208	388	8	showed	show	VERB
eurjchem-208	388	9	low	low	ADJ
eurjchem-208	388	10	activity	activity	NOUN
eurjchem-208	388	11	at	at	ADP
eurjchem-208	388	12	1	1	NUM
eurjchem-208	388	13	mg	mg	PROPN
eurjchem-208	388	14	/	/	SYM
eurjchem-208	388	15	cm3	cm3	NOUN
eurjchem-208	388	16	and	and	CCONJ
eurjchem-208	388	17	moderate	moderate	ADJ
eurjchem-208	388	18	inhibition	inhibition	NOUN
eurjchem-208	388	19	at	at	ADP
eurjchem-208	388	20	2	2	NUM
eurjchem-208	388	21	mg	mg	PROPN
eurjchem-208	388	22	/	/	SYM
eurjchem-208	388	23	cm3	cm3	NOUN
eurjchem-208	388	24	.	.	NOUN
eurjchem-208	388	25	5	5	NUM
eurjchem-208	388	26	)	)	PUNCT
eurjchem-208	388	27	phosphonicdihydrazones	phosphonicdihydrazone	NOUN
eurjchem-208	389	1	3a‐d	3a‐d	ADV
eurjchem-208	389	2	did	do	AUX
eurjchem-208	389	3	not	not	PART
eurjchem-208	389	4	exhibit	exhibit	VERB
eurjchem-208	389	5	any	any	DET
eurjchem-208	389	6	effects	effect	NOUN
eurjchem-208	389	7	against	against	ADP
eurjchem-208	389	8	all	all	DET
eurjchem-208	389	9	microbial	microbial	ADJ
eurjchem-208	389	10	strains	strain	NOUN
eurjchem-208	389	11	.	.	PUNCT
eurjchem-208	390	1	only	only	ADV
eurjchem-208	390	2	compound	compound	NOUN
eurjchem-208	390	3	3b	3b	NOUN
eurjchem-208	390	4	showed	show	VERB
eurjchem-208	390	5	a	a	DET
eurjchem-208	390	6	lower	low	ADJ
eurjchem-208	390	7	inhibition	inhibition	NOUN
eurjchem-208	390	8	against	against	ADP
eurjchem-208	390	9	gram‐negative	gram‐negative	ADJ
eurjchem-208	390	10	bacteria	bacteria	NOUN
eurjchem-208	390	11	at	at	ADP
eurjchem-208	390	12	2	2	NUM
eurjchem-208	390	13	mg	mg	PROPN
eurjchem-208	390	14	/	/	SYM
eurjchem-208	390	15	cm3	cm3	PROPN
eurjchem-208	390	16	.	.	PUNCT
eurjchem-208	390	17	table	table	NOUN
eurjchem-208	390	18	2	2	NUM
eurjchem-208	390	19	.	.	PUNCT
eurjchem-208	390	20	antibacterial	antibacterial	ADJ
eurjchem-208	390	21	activity	activity	NOUN
eurjchem-208	390	22	(	(	PUNCT
eurjchem-208	390	23	gram	gram	NOUN
eurjchem-208	390	24	negative	negative	ADJ
eurjchem-208	390	25	bacteria	bacteria	NOUN
eurjchem-208	390	26	)	)	PUNCT
eurjchem-208	390	27	of	of	ADP
eurjchem-208	390	28	the	the	DET
eurjchem-208	390	29	synthesized	synthesize	VERB
eurjchem-208	390	30	compounds	compound	NOUN
eurjchem-208	390	31	3−22	3−22	PROPN
eurjchem-208	390	32	at	at	ADP
eurjchem-208	390	33	1	1	NUM
eurjchem-208	390	34	and	and	CCONJ
eurjchem-208	390	35	2	2	NUM
eurjchem-208	390	36	mg	mg	NUM
eurjchem-208	390	37	/	/	SYM
eurjchem-208	390	38	cm3	cm3	NOUN
eurjchem-208	390	39	by	by	ADP
eurjchem-208	390	40	disc	disc	NOUN
eurjchem-208	390	41	diffusion	diffusion	NOUN
eurjchem-208	390	42	assay	assay	PROPN
eurjchem-208	390	43	*	*	PROPN
eurjchem-208	390	44	.	.	PUNCT
eurjchem-208	391	1	compound	compound	NOUN
eurjchem-208	391	2	diameter	diameter	NOUN
eurjchem-208	391	3	of	of	ADP
eurjchem-208	391	4	zone	zone	NOUN
eurjchem-208	391	5	of	of	ADP
eurjchem-208	391	6	inhibition	inhibition	NOUN
eurjchem-208	391	7	in	in	ADP
eurjchem-208	391	8	mm	mm	PROPN
eurjchem-208	391	9	gram‐negative	gram‐negative	PROPN
eurjchem-208	391	10	bacteria	bacteria	NOUN
eurjchem-208	391	11	p.	p.	PROPN
eurjchem-208	391	12	phaseolicola	phaseolicola	PROPN
eurjchem-208	391	13	(	(	PUNCT
eurjchem-208	391	14	gspb	gspb	NOUN
eurjchem-208	391	15	2828	2828	NUM
eurjchem-208	391	16	)	)	PUNCT
eurjchem-208	392	1	p.	p.	NOUN
eurjchem-208	392	2	fluorescens	fluorescen	NOUN
eurjchem-208	392	3	(	(	PUNCT
eurjchem-208	392	4	s	s	NOUN
eurjchem-208	392	5	97	97	NUM
eurjchem-208	392	6	)	)	SYM
eurjchem-208	392	7	2	2	NUM
eurjchem-208	392	8	mg	mg	PROPN
eurjchem-208	392	9	/	/	SYM
eurjchem-208	392	10	cm3	cm3	NOUN
eurjchem-208	392	11	1	1	NUM
eurjchem-208	392	12	mg	mg	NOUN
eurjchem-208	392	13	/	/	SYM
eurjchem-208	392	14	cm3	cm3	NOUN
eurjchem-208	392	15	2	2	NUM
eurjchem-208	392	16	mg	mg	PROPN
eurjchem-208	392	17	/	/	SYM
eurjchem-208	392	18	cm3	cm3	NOUN
eurjchem-208	392	19	1	1	NUM
eurjchem-208	392	20	mg	mg	NUM
eurjchem-208	392	21	/	/	SYM
eurjchem-208	392	22	cm3	cm3	PROPN
eurjchem-208	392	23	3a	3a	NUM
eurjchem-208	392	24	−	−	ADP
eurjchem-208	392	25	−	−	PROPN
eurjchem-208	392	26	−	−	PROPN
eurjchem-208	393	1	−	−	PROPN
eurjchem-208	393	2	3b	3b	NOUN
eurjchem-208	393	3	6	6	NUM
eurjchem-208	393	4	−	−	NOUN
eurjchem-208	393	5	7	7	NUM
eurjchem-208	393	6	−	−	PROPN
eurjchem-208	393	7	3c	3c	NUM
eurjchem-208	393	8	−	−	NOUN
eurjchem-208	393	9	−	−	PROPN
eurjchem-208	393	10	−	−	PROPN
eurjchem-208	393	11	−	−	PROPN
eurjchem-208	393	12	3d	3d	NOUN
eurjchem-208	393	13	−	−	PROPN
eurjchem-208	394	1	−	−	PROPN
eurjchem-208	395	1	−	−	PROPN
eurjchem-208	395	2	−	−	PROPN
eurjchem-208	395	3	4a	4a	NOUN
eurjchem-208	395	4	10	10	NUM
eurjchem-208	395	5	8	8	NUM
eurjchem-208	395	6	8	8	NUM
eurjchem-208	395	7	6	6	NUM
eurjchem-208	395	8	4b	4b	NOUN
eurjchem-208	396	1	−	−	NOUN
eurjchem-208	396	2	−	−	PROPN
eurjchem-208	396	3	6	6	NUM
eurjchem-208	396	4	−	−	NOUN
eurjchem-208	396	5	6	6	NUM
eurjchem-208	396	6	5	5	NUM
eurjchem-208	396	7	−	−	NOUN
eurjchem-208	396	8	7	7	NUM
eurjchem-208	396	9	−	−	NOUN
eurjchem-208	396	10	8	8	NUM
eurjchem-208	396	11	9	9	NUM
eurjchem-208	396	12	5	5	NUM
eurjchem-208	396	13	9	9	NUM
eurjchem-208	396	14	7	7	NUM
eurjchem-208	396	15	9	9	NUM
eurjchem-208	396	16	5	5	NUM
eurjchem-208	396	17	−	−	NOUN
eurjchem-208	396	18	6	6	NUM
eurjchem-208	396	19	−	−	NOUN
eurjchem-208	396	20	10	10	NUM
eurjchem-208	396	21	6	6	NUM
eurjchem-208	396	22	−	−	NUM
eurjchem-208	396	23	8	8	NUM
eurjchem-208	396	24	−	−	NOUN
eurjchem-208	396	25	11	11	NUM
eurjchem-208	396	26	7	7	NUM
eurjchem-208	396	27	6	6	NUM
eurjchem-208	396	28	10	10	NUM
eurjchem-208	396	29	7	7	NUM
eurjchem-208	396	30	12	12	NUM
eurjchem-208	396	31	10	10	NUM
eurjchem-208	396	32	7	7	NUM
eurjchem-208	396	33	8	8	NUM
eurjchem-208	396	34	6	6	NUM
eurjchem-208	396	35	14	14	NUM
eurjchem-208	396	36	13	13	NUM
eurjchem-208	396	37	10	10	NUM
eurjchem-208	396	38	9	9	NUM
eurjchem-208	396	39	6	6	NUM
eurjchem-208	396	40	16	16	NUM
eurjchem-208	396	41	12	12	NUM
eurjchem-208	396	42	10	10	NUM
eurjchem-208	396	43	12	12	NUM
eurjchem-208	396	44	9	9	NUM
eurjchem-208	396	45	18	18	NUM
eurjchem-208	396	46	6	6	NUM
eurjchem-208	396	47	−	−	NOUN
eurjchem-208	396	48	7	7	NUM
eurjchem-208	396	49	−	−	NOUN
eurjchem-208	396	50	20	20	NUM
eurjchem-208	396	51	27	27	NUM
eurjchem-208	396	52	22	22	NUM
eurjchem-208	396	53	20	20	NUM
eurjchem-208	396	54	12	12	NUM
eurjchem-208	396	55	22	22	NUM
eurjchem-208	396	56	20	20	NUM
eurjchem-208	396	57	14	14	NUM
eurjchem-208	396	58	24	24	NUM
eurjchem-208	396	59	18	18	NUM
eurjchem-208	396	60	chloramphenicol	chloramphenicol	NOUN
eurjchem-208	396	61	25	25	NUM
eurjchem-208	396	62	30	30	NUM
eurjchem-208	396	63	*	*	SYM
eurjchem-208	396	64	less	less	ADV
eurjchem-208	396	65	active	active	ADJ
eurjchem-208	396	66	:	:	PUNCT
eurjchem-208	396	67	6‐12	6‐12	NUM
eurjchem-208	396	68	mm	mm	INTJ
eurjchem-208	396	69	;	;	PUNCT
eurjchem-208	396	70	moderately	moderately	ADV
eurjchem-208	396	71	active	active	ADJ
eurjchem-208	396	72	:	:	PUNCT
eurjchem-208	396	73	13‐19	13‐19	NUM
eurjchem-208	396	74	mm	mm	NOUN
eurjchem-208	396	75	;	;	PUNCT
eurjchem-208	396	76	highly	highly	ADV
eurjchem-208	396	77	active	active	ADJ
eurjchem-208	396	78	:	:	PUNCT
eurjchem-208	396	79	20‐30	20‐30	PROPN
eurjchem-208	396	80	mm	mm	INTJ
eurjchem-208	396	81	;	;	PUNCT
eurjchem-208	396	82	–	–	PUNCT
eurjchem-208	396	83	:	:	PUNCT
eurjchem-208	396	84	no	no	DET
eurjchem-208	396	85	inhibition	inhibition	NOUN
eurjchem-208	396	86	or	or	CCONJ
eurjchem-208	396	87	inhibition	inhibition	NOUN
eurjchem-208	396	88	less	less	ADJ
eurjchem-208	396	89	than	than	ADP
eurjchem-208	396	90	5	5	NUM
eurjchem-208	396	91	mm	mm	NOUN
eurjchem-208	396	92	.	.	NOUN
eurjchem-208	396	93	table	table	NOUN
eurjchem-208	396	94	3	3	NUM
eurjchem-208	396	95	.	.	PUNCT
eurjchem-208	396	96	antifungal	antifungal	ADJ
eurjchem-208	396	97	activity	activity	NOUN
eurjchem-208	396	98	of	of	ADP
eurjchem-208	396	99	the	the	DET
eurjchem-208	396	100	synthesized	synthesize	VERB
eurjchem-208	396	101	compounds	compound	NOUN
eurjchem-208	396	102	3−22	3−22	PROPN
eurjchem-208	396	103	at	at	ADP
eurjchem-208	396	104	1	1	NUM
eurjchem-208	396	105	and	and	CCONJ
eurjchem-208	396	106	2	2	NUM
eurjchem-208	396	107	mg	mg	NUM
eurjchem-208	396	108	/	/	SYM
eurjchem-208	396	109	cm3	cm3	NOUN
eurjchem-208	396	110	by	by	ADP
eurjchem-208	396	111	disc	disc	NOUN
eurjchem-208	396	112	diffusion	diffusion	NOUN
eurjchem-208	396	113	assay	assay	PROPN
eurjchem-208	396	114	*	*	PROPN
eurjchem-208	396	115	.	.	PUNCT
eurjchem-208	397	1	compound	compound	NOUN
eurjchem-208	397	2	diameter	diameter	NOUN
eurjchem-208	397	3	of	of	ADP
eurjchem-208	397	4	zone	zone	NOUN
eurjchem-208	397	5	of	of	ADP
eurjchem-208	397	6	inhibition	inhibition	NOUN
eurjchem-208	397	7	in	in	ADP
eurjchem-208	397	8	mm	mm	PROPN
eurjchem-208	397	9	fungi	fungi	PROPN
eurjchem-208	397	10	f.	f.	PROPN
eurjchem-208	397	11	oxysporum	oxysporum	PROPN
eurjchem-208	397	12	a.	a.	PROPN
eurjchem-208	397	13	fumigatus	fumigatus	NOUN
eurjchem-208	397	14	2	2	NUM
eurjchem-208	397	15	mg	mg	NUM
eurjchem-208	397	16	/	/	SYM
eurjchem-208	397	17	cm3	cm3	NOUN
eurjchem-208	397	18	1	1	NUM
eurjchem-208	397	19	mg	mg	NOUN
eurjchem-208	397	20	/	/	SYM
eurjchem-208	397	21	cm3	cm3	NOUN
eurjchem-208	397	22	2	2	NUM
eurjchem-208	397	23	mg	mg	PROPN
eurjchem-208	397	24	/	/	SYM
eurjchem-208	397	25	cm3	cm3	NOUN
eurjchem-208	397	26	1	1	NUM
eurjchem-208	397	27	mg	mg	NUM
eurjchem-208	397	28	/	/	SYM
eurjchem-208	397	29	cm3	cm3	PROPN
eurjchem-208	397	30	3a	3a	NUM
eurjchem-208	397	31	−	−	ADP
eurjchem-208	397	32	−	−	PROPN
eurjchem-208	398	1	−	−	PROPN
eurjchem-208	398	2	−	−	PROPN
eurjchem-208	398	3	3b	3b	NOUN
eurjchem-208	398	4	−	−	NOUN
eurjchem-208	399	1	−	−	NOUN
eurjchem-208	400	1	−	−	PROPN
eurjchem-208	401	1	−	−	PROPN
eurjchem-208	402	1	3c	3c	NUM
eurjchem-208	402	2	−	−	NOUN
eurjchem-208	402	3	−	−	PROPN
eurjchem-208	403	1	−	−	PROPN
eurjchem-208	403	2	−	−	PROPN
eurjchem-208	404	1	3d	3d	NOUN
eurjchem-208	404	2	−	−	PROPN
eurjchem-208	405	1	−	−	PROPN
eurjchem-208	406	1	−	−	PROPN
eurjchem-208	406	2	−	−	PROPN
eurjchem-208	406	3	4a	4a	NOUN
eurjchem-208	406	4	−	−	NOUN
eurjchem-208	407	1	−	−	NOUN
eurjchem-208	408	1	−	−	NUM
eurjchem-208	408	2	6	6	NUM
eurjchem-208	408	3	4b	4b	NOUN
eurjchem-208	408	4	−	−	PROPN
eurjchem-208	409	1	−	−	PROPN
eurjchem-208	410	1	−	−	NOUN
eurjchem-208	411	1	−	−	NUM
eurjchem-208	411	2	6	6	NUM
eurjchem-208	411	3	−	−	NOUN
eurjchem-208	411	4	−	−	PROPN
eurjchem-208	411	5	−	−	NOUN
eurjchem-208	412	1	−	−	NUM
eurjchem-208	412	2	8	8	NUM
eurjchem-208	412	3	−	−	NOUN
eurjchem-208	412	4	−	−	NOUN
eurjchem-208	412	5	−	−	NUM
eurjchem-208	412	6	7	7	NUM
eurjchem-208	412	7	9	9	NUM
eurjchem-208	412	8	−	−	NUM
eurjchem-208	412	9	−	−	PROPN
eurjchem-208	412	10	−	−	NOUN
eurjchem-208	413	1	−	−	NUM
eurjchem-208	413	2	10	10	NUM
eurjchem-208	413	3	−	−	NOUN
eurjchem-208	413	4	−	−	NOUN
eurjchem-208	413	5	−	−	NOUN
eurjchem-208	414	1	−	−	NUM
eurjchem-208	414	2	11	11	NUM
eurjchem-208	414	3	17	17	NUM
eurjchem-208	414	4	10	10	NUM
eurjchem-208	414	5	14	14	NUM
eurjchem-208	414	6	7	7	NUM
eurjchem-208	414	7	12	12	NUM
eurjchem-208	414	8	−	−	NOUN
eurjchem-208	414	9	−	−	NOUN
eurjchem-208	414	10	−	−	NUM
eurjchem-208	414	11	6	6	NUM
eurjchem-208	414	12	14	14	NUM
eurjchem-208	414	13	8	8	NUM
eurjchem-208	414	14	−	−	NOUN
eurjchem-208	414	15	−	−	NUM
eurjchem-208	414	16	6	6	NUM
eurjchem-208	414	17	16	16	NUM
eurjchem-208	414	18	11	11	NUM
eurjchem-208	414	19	9	9	NUM
eurjchem-208	414	20	7	7	NUM
eurjchem-208	414	21	9	9	NUM
eurjchem-208	414	22	18	18	NUM
eurjchem-208	414	23	−	−	NUM
eurjchem-208	414	24	−	−	PROPN
eurjchem-208	414	25	−	−	NOUN
eurjchem-208	415	1	−	−	NUM
eurjchem-208	415	2	20	20	NUM
eurjchem-208	415	3	−	−	NOUN
eurjchem-208	415	4	−	−	NOUN
eurjchem-208	416	1	−	−	NUM
eurjchem-208	416	2	12	12	NUM
eurjchem-208	416	3	22	22	NUM
eurjchem-208	416	4	35	35	NUM
eurjchem-208	416	5	29	29	NUM
eurjchem-208	416	6	33	33	NUM
eurjchem-208	416	7	18	18	NUM
eurjchem-208	416	8	cycloheximide	cycloheximide	NOUN
eurjchem-208	416	9	28	28	NUM
eurjchem-208	416	10	31	31	NUM
eurjchem-208	416	11	*	*	PUNCT
eurjchem-208	416	12	less	less	ADV
eurjchem-208	416	13	active	active	ADJ
eurjchem-208	416	14	:	:	PUNCT
eurjchem-208	416	15	6‐12	6‐12	NUM
eurjchem-208	416	16	mm	mm	INTJ
eurjchem-208	416	17	;	;	PUNCT
eurjchem-208	416	18	moderately	moderately	ADV
eurjchem-208	416	19	active	active	ADJ
eurjchem-208	416	20	:	:	PUNCT
eurjchem-208	416	21	13‐19	13‐19	NUM
eurjchem-208	416	22	mm	mm	NOUN
eurjchem-208	416	23	;	;	PUNCT
eurjchem-208	416	24	highly	highly	ADV
eurjchem-208	416	25	active	active	ADJ
eurjchem-208	416	26	:	:	PUNCT
eurjchem-208	416	27	20‐30	20‐30	PROPN
eurjchem-208	416	28	mm	mm	INTJ
eurjchem-208	416	29	;	;	PUNCT
eurjchem-208	416	30	–	–	PUNCT
eurjchem-208	416	31	:	:	PUNCT
eurjchem-208	416	32	no	no	DET
eurjchem-208	416	33	inhibition	inhibition	NOUN
eurjchem-208	416	34	or	or	CCONJ
eurjchem-208	416	35	inhibition	inhibition	NOUN
eurjchem-208	416	36	less	less	ADJ
eurjchem-208	416	37	than	than	ADP
eurjchem-208	416	38	5	5	NUM
eurjchem-208	416	39	mm	mm	NOUN
eurjchem-208	416	40	.	.	PROPN
eurjchem-208	416	41	6	6	NUM
eurjchem-208	416	42	)	)	PUNCT
eurjchem-208	416	43	the	the	DET
eurjchem-208	416	44	products	product	NOUN
eurjchem-208	416	45	4a	4a	NOUN
eurjchem-208	416	46	,	,	PUNCT
eurjchem-208	416	47	b	b	NOUN
eurjchem-208	416	48	,	,	PUNCT
eurjchem-208	416	49	6	6	NUM
eurjchem-208	416	50	and	and	CCONJ
eurjchem-208	416	51	8	8	NUM
eurjchem-208	416	52	revealed	reveal	VERB
eurjchem-208	416	53	better	well	ADJ
eurjchem-208	416	54	activities	activity	NOUN
eurjchem-208	416	55	against	against	ADP
eurjchem-208	416	56	bacterial	bacterial	ADJ
eurjchem-208	416	57	strains	strain	NOUN
eurjchem-208	416	58	in	in	ADP
eurjchem-208	416	59	comparison	comparison	NOUN
eurjchem-208	416	60	with	with	ADP
eurjchem-208	416	61	the	the	DET
eurjchem-208	416	62	corresponding	correspond	VERB
eurjchem-208	416	63	phosphonicdihydrazones	phosphonicdihydrazone	NOUN
eurjchem-208	416	64	3a‐d	3a‐d	ADV
eurjchem-208	416	65	.	.	PUNCT
eurjchem-208	417	1	this	this	DET
eurjchem-208	417	2	activity	activity	NOUN
eurjchem-208	417	3	may	may	AUX
eurjchem-208	417	4	be	be	AUX
eurjchem-208	417	5	attributed	attribute	VERB
eurjchem-208	417	6	to	to	ADP
eurjchem-208	417	7	the	the	DET
eurjchem-208	417	8	presence	presence	NOUN
eurjchem-208	417	9	of	of	ADP
eurjchem-208	417	10	the	the	DET
eurjchem-208	417	11	formed	form	VERB
eurjchem-208	417	12	bioactive	bioactive	PROPN
eurjchem-208	417	13	pyrazole	pyrazole	NOUN
eurjchem-208	417	14	rings	ring	NOUN
eurjchem-208	417	15	by	by	ADP
eurjchem-208	417	16	vilsmeier‐haack	vilsmeier‐haack	NOUN
eurjchem-208	417	17	reaction	reaction	NOUN
eurjchem-208	417	18	.	.	PUNCT
eurjchem-208	418	1	7	7	X
eurjchem-208	418	2	)	)	PUNCT
eurjchem-208	418	3	compounds	compound	VERB
eurjchem-208	418	4	9	9	NUM
eurjchem-208	418	5	,	,	PUNCT
eurjchem-208	418	6	12	12	NUM
eurjchem-208	418	7	and	and	CCONJ
eurjchem-208	418	8	18	18	NUM
eurjchem-208	418	9	did	do	AUX
eurjchem-208	418	10	not	not	PART
eurjchem-208	418	11	show	show	VERB
eurjchem-208	418	12	noticeable	noticeable	ADJ
eurjchem-208	418	13	activity	activity	NOUN
eurjchem-208	418	14	in	in	ADP
eurjchem-208	418	15	comparison	comparison	NOUN
eurjchem-208	418	16	with	with	ADP
eurjchem-208	418	17	their	their	PRON
eurjchem-208	418	18	corresponding	corresponding	ADJ
eurjchem-208	418	19	bis(4‐	bis(4‐	PROPN
eurjchem-208	418	20	formylpyrazolyl	formylpyrazolyl	NOUN
eurjchem-208	418	21	)	)	PUNCT
eurjchem-208	418	22	phosphine	phosphine	NOUN
eurjchem-208	418	23	oxides	oxide	NOUN
eurjchem-208	418	24	4a	4a	NOUN
eurjchem-208	418	25	and	and	CCONJ
eurjchem-208	418	26	4b	4b	PROPN
eurjchem-208	418	27	(	(	PUNCT
eurjchem-208	418	28	figures	figure	VERB
eurjchem-208	418	29	1‐3	1‐3	PROPN
eurjchem-208	418	30	)	)	PUNCT
eurjchem-208	418	31	.	.	PUNCT
eurjchem-208	419	1	8)	8)	NUM
eurjchem-208	419	2	compounds	compound	NOUN
eurjchem-208	419	3	10	10	NUM
eurjchem-208	419	4	,	,	PUNCT
eurjchem-208	419	5	14	14	NUM
eurjchem-208	419	6	and	and	CCONJ
eurjchem-208	419	7	20	20	NUM
eurjchem-208	419	8	showed	show	VERB
eurjchem-208	419	9	slightly	slightly	ADJ
eurjchem-208	419	10	activity	activity	NOUN
eurjchem-208	419	11	more	more	ADJ
eurjchem-208	419	12	than	than	ADP
eurjchem-208	419	13	their	their	PRON
eurjchem-208	419	14	corresponding	correspond	VERB
eurjchem-208	419	15	starting	starting	NOUN
eurjchem-208	419	16	material	material	NOUN
eurjchem-208	419	17	9	9	NUM
eurjchem-208	419	18	,	,	PUNCT
eurjchem-208	419	19	12	12	NUM
eurjchem-208	419	20	and	and	CCONJ
eurjchem-208	419	21	18	18	NUM
eurjchem-208	419	22	,	,	PUNCT
eurjchem-208	419	23	respectively	respectively	ADV
eurjchem-208	419	24	,	,	PUNCT
eurjchem-208	419	25	as	as	ADP
eurjchem-208	419	26	result	result	NOUN
eurjchem-208	419	27	of	of	ADP
eurjchem-208	419	28	sulfur	sulfur	NOUN
eurjchem-208	419	29	atoms	atom	NOUN
eurjchem-208	419	30	effects	effect	NOUN
eurjchem-208	419	31	to	to	ADP
eurjchem-208	419	32	their	their	PRON
eurjchem-208	419	33	structures	structure	NOUN
eurjchem-208	419	34	,	,	PUNCT
eurjchem-208	419	35	which	which	PRON
eurjchem-208	419	36	may	may	AUX
eurjchem-208	419	37	cause	cause	VERB
eurjchem-208	419	38	enhanced	enhanced	ADJ
eurjchem-208	419	39	activity	activity	NOUN
eurjchem-208	419	40	(	(	PUNCT
eurjchem-208	419	41	figures	figure	NOUN
eurjchem-208	419	42	1‐3	1‐3	PROPN
eurjchem-208	419	43	)	)	PUNCT
eurjchem-208	419	44	.	.	PUNCT
eurjchem-208	420	1	9	9	X
eurjchem-208	420	2	)	)	PUNCT
eurjchem-208	420	3	compounds	compound	VERB
eurjchem-208	420	4	11	11	NUM
eurjchem-208	420	5	,	,	PUNCT
eurjchem-208	420	6	16	16	NUM
eurjchem-208	420	7	and	and	CCONJ
eurjchem-208	420	8	22	22	NUM
eurjchem-208	420	9	showed	show	VERB
eurjchem-208	420	10	comparatively	comparatively	ADV
eurjchem-208	420	11	good	good	ADJ
eurjchem-208	420	12	activity	activity	NOUN
eurjchem-208	420	13	more	more	ADJ
eurjchem-208	420	14	than	than	ADP
eurjchem-208	420	15	their	their	PRON
eurjchem-208	420	16	corresponding	correspond	VERB
eurjchem-208	420	17	starting	starting	NOUN
eurjchem-208	420	18	material	material	NOUN
eurjchem-208	420	19	9	9	NUM
eurjchem-208	420	20	,	,	PUNCT
eurjchem-208	420	21	12	12	NUM
eurjchem-208	420	22	and	and	CCONJ
eurjchem-208	420	23	18	18	NUM
eurjchem-208	420	24	,	,	PUNCT
eurjchem-208	420	25	respectively	respectively	ADV
eurjchem-208	420	26	,	,	PUNCT
eurjchem-208	420	27	which	which	PRON
eurjchem-208	420	28	may	may	AUX
eurjchem-208	420	29	due	due	ADP
eurjchem-208	420	30	to	to	ADP
eurjchem-208	420	31	addition	addition	NOUN
eurjchem-208	420	32	phosphorus	phosphorus	NOUN
eurjchem-208	420	33	atoms	atom	NOUN
eurjchem-208	420	34	to	to	ADP
eurjchem-208	420	35	their	their	PRON
eurjchem-208	420	36	structures	structure	NOUN
eurjchem-208	420	37	which	which	PRON
eurjchem-208	420	38	may	may	AUX
eurjchem-208	420	39	cause	cause	VERB
eurjchem-208	420	40	enhanced	enhanced	ADJ
eurjchem-208	420	41	activity	activity	NOUN
eurjchem-208	420	42	(	(	PUNCT
eurjchem-208	420	43	figures	figure	NOUN
eurjchem-208	420	44	1‐3	1‐3	PROPN
eurjchem-208	420	45	)	)	PUNCT
eurjchem-208	420	46	.	.	PUNCT
eurjchem-208	421	1	10	10	NUM
eurjchem-208	421	2	)	)	PUNCT
eurjchem-208	421	3	compounds	compound	VERB
eurjchem-208	421	4	11	11	NUM
eurjchem-208	421	5	,	,	PUNCT
eurjchem-208	421	6	16	16	NUM
eurjchem-208	421	7	and	and	CCONJ
eurjchem-208	421	8	22	22	NUM
eurjchem-208	421	9	(	(	PUNCT
eurjchem-208	421	10	including	include	VERB
eurjchem-208	421	11	extra	extra	ADJ
eurjchem-208	421	12	phosphorus	phosphorus	NOUN
eurjchem-208	421	13	atom	atom	NOUN
eurjchem-208	421	14	)	)	PUNCT
eurjchem-208	421	15	showed	show	VERB
eurjchem-208	421	16	good	good	ADJ
eurjchem-208	421	17	inhibitions	inhibition	NOUN
eurjchem-208	421	18	against	against	ADP
eurjchem-208	421	19	all	all	DET
eurjchem-208	421	20	bacterial	bacterial	ADJ
eurjchem-208	421	21	and	and	CCONJ
eurjchem-208	421	22	fungal	fungal	ADJ
eurjchem-208	421	23	strains	strain	NOUN
eurjchem-208	421	24	,	,	PUNCT
eurjchem-208	421	25	while	while	SCONJ
eurjchem-208	421	26	compounds	compound	NOUN
eurjchem-208	421	27	10	10	NUM
eurjchem-208	421	28	,	,	PUNCT
eurjchem-208	421	29	14	14	NUM
eurjchem-208	421	30	and	and	CCONJ
eurjchem-208	421	31	20	20	NUM
eurjchem-208	421	32	(	(	PUNCT
eurjchem-208	421	33	including	include	VERB
eurjchem-208	421	34	sulfur	sulfur	NOUN
eurjchem-208	421	35	atom	atom	NOUN
eurjchem-208	421	36	)	)	PUNCT
eurjchem-208	421	37	showed	show	VERB
eurjchem-208	421	38	a	a	DET
eurjchem-208	421	39	degree	degree	NOUN
eurjchem-208	421	40	of	of	ADP
eurjchem-208	421	41	inhibition	inhibition	NOUN
eurjchem-208	421	42	against	against	ADP
eurjchem-208	421	43	only	only	ADJ
eurjchem-208	421	44	bacterial	bacterial	ADJ
eurjchem-208	421	45	strains	strain	NOUN
eurjchem-208	421	46	(	(	PUNCT
eurjchem-208	421	47	tables	table	NOUN
eurjchem-208	421	48	1	1	NUM
eurjchem-208	421	49	and	and	CCONJ
eurjchem-208	421	50	2	2	NUM
eurjchem-208	421	51	)	)	PUNCT
eurjchem-208	421	52	.	.	PUNCT
eurjchem-208	422	1	this	this	PRON
eurjchem-208	422	2	may	may	AUX
eurjchem-208	422	3	be	be	AUX
eurjchem-208	422	4	due	due	ADJ
eurjchem-208	422	5	to	to	ADP
eurjchem-208	422	6	a	a	DET
eurjchem-208	422	7	combination	combination	NOUN
eurjchem-208	422	8	34	34	NUM
eurjchem-208	422	9	abdel‐aziz	abdel‐aziz	INTJ
eurjchem-208	422	10	et	et	PROPN
eurjchem-208	422	11	al	al	PROPN
eurjchem-208	422	12	.	.	PUNCT
eurjchem-208	422	13	/	/	SYM
eurjchem-208	422	14	european	european	PROPN
eurjchem-208	422	15	journal	journal	PROPN
eurjchem-208	422	16	of	of	ADP
eurjchem-208	422	17	chemistry	chemistry	NOUN
eurjchem-208	422	18	2	2	NUM
eurjchem-208	422	19	(	(	PUNCT
eurjchem-208	422	20	1	1	NUM
eurjchem-208	422	21	)	)	PUNCT
eurjchem-208	422	22	(	(	PUNCT
eurjchem-208	422	23	2011	2011	NUM
eurjchem-208	422	24	)	)	PUNCT
eurjchem-208	422	25	25‐35	25‐35	NUM
eurjchem-208	422	26	between	between	ADP
eurjchem-208	422	27	the	the	DET
eurjchem-208	422	28	extra	extra	ADJ
eurjchem-208	422	29	phosphorus	phosphorus	NOUN
eurjchem-208	422	30	atoms	atom	NOUN
eurjchem-208	422	31	withcompounds	withcompound	VERB
eurjchem-208	422	32	9	9	NUM
eurjchem-208	422	33	,	,	PUNCT
eurjchem-208	422	34	12	12	NUM
eurjchem-208	422	35	and	and	CCONJ
eurjchem-208	422	36	18	18	NUM
eurjchem-208	422	37	leading	lead	VERB
eurjchem-208	422	38	to	to	ADP
eurjchem-208	422	39	a	a	DET
eurjchem-208	422	40	biocidal	biocidal	ADJ
eurjchem-208	422	41	effects	effect	NOUN
eurjchem-208	422	42	activity	activity	NOUN
eurjchem-208	422	43	more	more	ADV
eurjchem-208	422	44	that	that	SCONJ
eurjchem-208	422	45	sulfur	sulfur	NOUN
eurjchem-208	422	46	atom	atom	NOUN
eurjchem-208	422	47	moieties	moiety	NOUN
eurjchem-208	422	48	.	.	PUNCT
eurjchem-208	423	1	11	11	NUM
eurjchem-208	423	2	)	)	PUNCT
eurjchem-208	423	3	compounds	compound	VERB
eurjchem-208	423	4	11	11	NUM
eurjchem-208	423	5	,	,	PUNCT
eurjchem-208	423	6	16	16	NUM
eurjchem-208	423	7	and	and	CCONJ
eurjchem-208	423	8	22	22	NUM
eurjchem-208	423	9	exhibited	exhibit	VERB
eurjchem-208	423	10	good	good	ADJ
eurjchem-208	423	11	inhibitions	inhibition	NOUN
eurjchem-208	423	12	against	against	ADP
eurjchem-208	423	13	all	all	DET
eurjchem-208	423	14	microbial	microbial	ADJ
eurjchem-208	423	15	strains	strain	NOUN
eurjchem-208	423	16	,	,	PUNCT
eurjchem-208	423	17	which	which	PRON
eurjchem-208	423	18	may	may	AUX
eurjchem-208	423	19	be	be	AUX
eurjchem-208	423	20	due	due	ADJ
eurjchem-208	423	21	to	to	ADP
eurjchem-208	423	22	presence	presence	NOUN
eurjchem-208	423	23	of	of	ADP
eurjchem-208	423	24	acyclic	acyclic	ADJ
eurjchem-208	423	25	or	or	CCONJ
eurjchem-208	423	26	cyclic	cyclic	ADJ
eurjchem-208	423	27	‐aminophosphonate	‐aminophosphonate	NOUN
eurjchem-208	423	28	and	and	CCONJ
eurjchem-208	423	29	ethyl	ethyl	PROPN
eurjchem-208	423	30	phosphonate	phosphonate	NOUN
eurjchem-208	423	31	moieties	moiety	NOUN
eurjchem-208	423	32	,	,	PUNCT
eurjchem-208	423	33	previously	previously	ADV
eurjchem-208	423	34	noted	note	VERB
eurjchem-208	423	35	for	for	ADP
eurjchem-208	423	36	their	their	PRON
eurjchem-208	423	37	impact	impact	NOUN
eurjchem-208	423	38	on	on	ADP
eurjchem-208	423	39	biological	biological	ADJ
eurjchem-208	423	40	systems	system	NOUN
eurjchem-208	423	41	[	[	X
eurjchem-208	423	42	17	17	NUM
eurjchem-208	423	43	]	]	PUNCT
eurjchem-208	423	44	(	(	PUNCT
eurjchem-208	423	45	figure	figure	NOUN
eurjchem-208	423	46	4	4	NUM
eurjchem-208	423	47	)	)	PUNCT
eurjchem-208	423	48	.	.	PUNCT
eurjchem-208	424	1	12	12	NUM
eurjchem-208	424	2	)	)	PUNCT
eurjchem-208	424	3	in	in	ADP
eurjchem-208	424	4	conclusion	conclusion	NOUN
eurjchem-208	424	5	,	,	PUNCT
eurjchem-208	424	6	compounds	compound	VERB
eurjchem-208	424	7	11	11	NUM
eurjchem-208	424	8	,	,	PUNCT
eurjchem-208	424	9	16	16	NUM
eurjchem-208	424	10	and	and	CCONJ
eurjchem-208	424	11	22	22	NUM
eurjchem-208	424	12	are	be	AUX
eurjchem-208	424	13	nearly	nearly	ADV
eurjchem-208	424	14	as	as	ADV
eurjchem-208	424	15	active	active	ADJ
eurjchem-208	424	16	as	as	ADP
eurjchem-208	424	17	reference	reference	NOUN
eurjchem-208	424	18	drugs	drug	NOUN
eurjchem-208	424	19	against	against	ADP
eurjchem-208	424	20	some	some	DET
eurjchem-208	424	21	microbial	microbial	ADJ
eurjchem-208	424	22	strains	strain	NOUN
eurjchem-208	424	23	.	.	PUNCT
eurjchem-208	425	1	however	however	ADV
eurjchem-208	425	2	none	none	NOUN
eurjchem-208	425	3	of	of	ADP
eurjchem-208	425	4	the	the	DET
eurjchem-208	425	5	test	test	NOUN
eurjchem-208	425	6	compounds	compound	NOUN
eurjchem-208	425	7	show	show	VERB
eurjchem-208	425	8	superior	superior	ADJ
eurjchem-208	425	9	activity	activity	NOUN
eurjchem-208	425	10	than	than	ADP
eurjchem-208	425	11	the	the	DET
eurjchem-208	425	12	reference	reference	NOUN
eurjchem-208	425	13	drugs	drug	NOUN
eurjchem-208	425	14	.	.	PUNCT
eurjchem-208	426	1	0	0	NUM
eurjchem-208	426	2	5	5	NUM
eurjchem-208	426	3	10	10	NUM
eurjchem-208	426	4	15	15	NUM
eurjchem-208	426	5	20	20	NUM
eurjchem-208	426	6	25	25	NUM
eurjchem-208	426	7	s.	s.	PROPN
eurjchem-208	426	8	aureus	aureus	PROPN
eurjchem-208	426	9	s.	s.	PROPN
eurjchem-208	426	10	pyogenes	pyogenes	PROPN
eurjchem-208	426	11	p.	p.	PROPN
eurjchem-208	426	12	phaseolicola	phaseolicola	PROPN
eurjchem-208	426	13	p.fluorescens	p.fluorescen	VERB
eurjchem-208	426	14	bacterial	bacterial	ADJ
eurjchem-208	426	15	strains	strain	NOUN
eurjchem-208	426	16	in	in	ADP
eurjchem-208	426	17	h	h	NOUN
eurjchem-208	426	18	ib	ib	NOUN
eurjchem-208	426	19	it	it	PRON
eurjchem-208	426	20	io	io	PROPN
eurjchem-208	426	21	n	n	ADV
eurjchem-208	426	22	z	z	NOUN
eurjchem-208	426	23	o	o	NOUN
eurjchem-208	427	1	n	n	X
eurjchem-208	427	2	e	e	X
eurjchem-208	427	3	s	s	X
eurjchem-208	427	4	(	(	PUNCT
eurjchem-208	427	5	m	m	VERB
eurjchem-208	427	6	m	m	VERB
eurjchem-208	427	7	)	)	PUNCT
eurjchem-208	427	8	a	a	DET
eurjchem-208	427	9	t	t	NOUN
eurjchem-208	427	10	2	2	NUM
eurjchem-208	427	11	m	m	NOUN
eurjchem-208	427	12	g	g	NOUN
eurjchem-208	427	13	/m	/m	PUNCT
eurjchem-208	427	14	l	l	NOUN
eurjchem-208	427	15	compound	compound	NOUN
eurjchem-208	427	16	4a	4a	NOUN
eurjchem-208	427	17	compound	compound	NOUN
eurjchem-208	427	18	9	9	NUM
eurjchem-208	427	19	compound	compound	NOUN
eurjchem-208	427	20	10	10	NUM
eurjchem-208	427	21	compound	compound	NOUN
eurjchem-208	427	22	11	11	NUM
eurjchem-208	427	23	figure	figure	NOUN
eurjchem-208	427	24	1	1	NUM
eurjchem-208	427	25	.	.	PUNCT
eurjchem-208	427	26	relationship	relationship	NOUN
eurjchem-208	427	27	between	between	ADP
eurjchem-208	427	28	inhibition	inhibition	NOUN
eurjchem-208	427	29	zones	zone	NOUN
eurjchem-208	427	30	at	at	ADP
eurjchem-208	427	31	2	2	NUM
eurjchem-208	427	32	mg	mg	NUM
eurjchem-208	427	33	/	/	SYM
eurjchem-208	427	34	ml	ml	NOUN
eurjchem-208	427	35	and	and	CCONJ
eurjchem-208	427	36	bacterial	bacterial	ADJ
eurjchem-208	427	37	strains	strain	NOUN
eurjchem-208	427	38	for	for	ADP
eurjchem-208	427	39	compounds	compound	NOUN
eurjchem-208	427	40	10	10	NUM
eurjchem-208	427	41	and	and	CCONJ
eurjchem-208	427	42	11	11	NUM
eurjchem-208	427	43	which	which	PRON
eurjchem-208	427	44	refers	refer	VERB
eurjchem-208	427	45	to	to	ADP
eurjchem-208	427	46	an	an	DET
eurjchem-208	427	47	increase	increase	NOUN
eurjchem-208	427	48	in	in	ADP
eurjchem-208	427	49	activity	activity	NOUN
eurjchem-208	427	50	via	via	ADP
eurjchem-208	427	51	addition	addition	NOUN
eurjchem-208	427	52	sulfur	sulfur	NOUN
eurjchem-208	427	53	and	and	CCONJ
eurjchem-208	427	54	phosphorus	phosphorus	NOUN
eurjchem-208	427	55	atoms	atom	NOUN
eurjchem-208	427	56	to	to	ADP
eurjchem-208	427	57	starting	start	VERB
eurjchem-208	427	58	materials	material	NOUN
eurjchem-208	427	59	4a	4a	NOUN
eurjchem-208	427	60	and	and	CCONJ
eurjchem-208	427	61	9	9	NUM
eurjchem-208	427	62	.	.	NOUN
eurjchem-208	427	63	0	0	NUM
eurjchem-208	427	64	5	5	NUM
eurjchem-208	427	65	10	10	NUM
eurjchem-208	427	66	15	15	NUM
eurjchem-208	427	67	20	20	NUM
eurjchem-208	427	68	25	25	NUM
eurjchem-208	427	69	30	30	NUM
eurjchem-208	427	70	s.	s.	PROPN
eurjchem-208	427	71	aureus	aureus	PROPN
eurjchem-208	427	72	s.	s.	PROPN
eurjchem-208	427	73	pyogenes	pyogenes	PROPN
eurjchem-208	428	1	p.	p.	PROPN
eurjchem-208	428	2	phaseolicola	phaseolicola	PROPN
eurjchem-208	429	1	p.	p.	NOUN
eurjchem-208	429	2	fluorescens	fluorescen	NOUN
eurjchem-208	430	1	bacterial	bacterial	ADJ
eurjchem-208	430	2	strains	strain	NOUN
eurjchem-208	430	3	in	in	ADP
eurjchem-208	430	4	h	h	NOUN
eurjchem-208	430	5	ib	ib	NOUN
eurjchem-208	430	6	it	it	PRON
eurjchem-208	430	7	io	io	PROPN
eurjchem-208	430	8	n	n	ADV
eurjchem-208	430	9	z	z	NOUN
eurjchem-208	430	10	o	o	NOUN
eurjchem-208	431	1	n	n	X
eurjchem-208	431	2	e	e	X
eurjchem-208	431	3	s	s	X
eurjchem-208	431	4	(	(	PUNCT
eurjchem-208	431	5	m	m	VERB
eurjchem-208	431	6	m	m	VERB
eurjchem-208	431	7	)	)	PUNCT
eurjchem-208	431	8	a	a	DET
eurjchem-208	431	9	t	t	NOUN
eurjchem-208	431	10	2	2	NUM
eurjchem-208	431	11	m	m	NOUN
eurjchem-208	431	12	g	g	NOUN
eurjchem-208	431	13	/m	/m	PUNCT
eurjchem-208	431	14	l	l	NOUN
eurjchem-208	431	15	compound	compound	NOUN
eurjchem-208	431	16	4a	4a	NOUN
eurjchem-208	431	17	compound	compound	NOUN
eurjchem-208	431	18	12	12	NUM
eurjchem-208	431	19	compound	compound	NOUN
eurjchem-208	431	20	14	14	NUM
eurjchem-208	431	21	compound	compound	NOUN
eurjchem-208	431	22	16	16	NUM
eurjchem-208	431	23	figure	figure	NOUN
eurjchem-208	431	24	2	2	NUM
eurjchem-208	431	25	.	.	X
eurjchem-208	431	26	relationship	relationship	NOUN
eurjchem-208	431	27	between	between	ADP
eurjchem-208	431	28	inhibition	inhibition	NOUN
eurjchem-208	431	29	zones	zone	NOUN
eurjchem-208	431	30	at	at	ADP
eurjchem-208	431	31	2	2	NUM
eurjchem-208	431	32	mg	mg	NUM
eurjchem-208	431	33	/	/	SYM
eurjchem-208	431	34	ml	ml	NOUN
eurjchem-208	431	35	and	and	CCONJ
eurjchem-208	431	36	bacterial	bacterial	ADJ
eurjchem-208	431	37	strains	strain	NOUN
eurjchem-208	431	38	for	for	ADP
eurjchem-208	431	39	compounds	compound	NOUN
eurjchem-208	431	40	14	14	NUM
eurjchem-208	431	41	and	and	CCONJ
eurjchem-208	431	42	16	16	NUM
eurjchem-208	431	43	which	which	PRON
eurjchem-208	431	44	refers	refer	VERB
eurjchem-208	431	45	to	to	ADP
eurjchem-208	431	46	an	an	DET
eurjchem-208	431	47	increase	increase	NOUN
eurjchem-208	431	48	in	in	ADP
eurjchem-208	431	49	activity	activity	NOUN
eurjchem-208	431	50	via	via	ADP
eurjchem-208	431	51	addition	addition	NOUN
eurjchem-208	431	52	sulfur	sulfur	NOUN
eurjchem-208	431	53	and	and	CCONJ
eurjchem-208	431	54	phosphorus	phosphorus	NOUN
eurjchem-208	431	55	atoms	atom	NOUN
eurjchem-208	431	56	to	to	ADP
eurjchem-208	431	57	starting	start	VERB
eurjchem-208	431	58	materials	material	NOUN
eurjchem-208	431	59	4a	4a	NOUN
eurjchem-208	431	60	and	and	CCONJ
eurjchem-208	431	61	12	12	NUM
eurjchem-208	431	62	.	.	NOUN
eurjchem-208	431	63	0	0	NUM
eurjchem-208	431	64	5	5	NUM
eurjchem-208	431	65	10	10	NUM
eurjchem-208	431	66	15	15	NUM
eurjchem-208	431	67	20	20	NUM
eurjchem-208	431	68	25	25	NUM
eurjchem-208	431	69	30	30	NUM
eurjchem-208	431	70	35	35	NUM
eurjchem-208	431	71	s.	s.	PROPN
eurjchem-208	431	72	aureus	aureus	PROPN
eurjchem-208	431	73	s.	s.	PROPN
eurjchem-208	431	74	pyogenes	pyogenes	PROPN
eurjchem-208	432	1	p.	p.	PROPN
eurjchem-208	432	2	phaseolicola	phaseolicola	PROPN
eurjchem-208	433	1	p.	p.	NOUN
eurjchem-208	433	2	fluorescens	fluorescen	NOUN
eurjchem-208	434	1	bacterial	bacterial	ADJ
eurjchem-208	434	2	strains	strain	NOUN
eurjchem-208	434	3	in	in	ADP
eurjchem-208	434	4	h	h	NOUN
eurjchem-208	434	5	ib	ib	NOUN
eurjchem-208	434	6	it	it	PRON
eurjchem-208	434	7	io	io	PROPN
eurjchem-208	434	8	n	n	ADV
eurjchem-208	434	9	z	z	NOUN
eurjchem-208	434	10	o	o	NOUN
eurjchem-208	435	1	n	n	X
eurjchem-208	435	2	e	e	X
eurjchem-208	435	3	s	s	X
eurjchem-208	435	4	(	(	PUNCT
eurjchem-208	435	5	m	m	VERB
eurjchem-208	435	6	m	m	VERB
eurjchem-208	435	7	)	)	PUNCT
eurjchem-208	435	8	a	a	DET
eurjchem-208	435	9	t	t	NOUN
eurjchem-208	435	10	2	2	NUM
eurjchem-208	435	11	m	m	NOUN
eurjchem-208	435	12	g	g	NOUN
eurjchem-208	435	13	/m	/m	PUNCT
eurjchem-208	435	14	l	l	PROPN
eurjchem-208	435	15	compound	compound	NOUN
eurjchem-208	435	16	4b	4b	PROPN
eurjchem-208	435	17	compound	compound	PROPN
eurjchem-208	435	18	18	18	NUM
eurjchem-208	435	19	compound	compound	NOUN
eurjchem-208	435	20	20	20	NUM
eurjchem-208	435	21	compound	compound	NOUN
eurjchem-208	435	22	22	22	NUM
eurjchem-208	435	23	figure	figure	NOUN
eurjchem-208	435	24	3	3	NUM
eurjchem-208	435	25	.	.	X
eurjchem-208	435	26	relationship	relationship	NOUN
eurjchem-208	435	27	between	between	ADP
eurjchem-208	435	28	inhibition	inhibition	NOUN
eurjchem-208	435	29	zones	zone	NOUN
eurjchem-208	435	30	at	at	ADP
eurjchem-208	435	31	2	2	NUM
eurjchem-208	435	32	mg	mg	NUM
eurjchem-208	435	33	/	/	SYM
eurjchem-208	435	34	ml	ml	NOUN
eurjchem-208	435	35	and	and	CCONJ
eurjchem-208	435	36	bacterial	bacterial	ADJ
eurjchem-208	435	37	strains	strain	NOUN
eurjchem-208	435	38	for	for	ADP
eurjchem-208	435	39	compounds	compound	NOUN
eurjchem-208	435	40	20	20	NUM
eurjchem-208	435	41	and	and	CCONJ
eurjchem-208	435	42	22	22	NUM
eurjchem-208	435	43	which	which	PRON
eurjchem-208	435	44	refers	refer	VERB
eurjchem-208	435	45	to	to	ADP
eurjchem-208	435	46	a	a	DET
eurjchem-208	435	47	clear	clear	ADJ
eurjchem-208	435	48	increase	increase	NOUN
eurjchem-208	435	49	in	in	ADP
eurjchem-208	435	50	activity	activity	NOUN
eurjchem-208	435	51	via	via	ADP
eurjchem-208	435	52	addition	addition	NOUN
eurjchem-208	435	53	sulfur	sulfur	NOUN
eurjchem-208	435	54	and	and	CCONJ
eurjchem-208	435	55	phosphorus	phosphorus	NOUN
eurjchem-208	435	56	atoms	atom	NOUN
eurjchem-208	435	57	to	to	ADP
eurjchem-208	435	58	starting	start	VERB
eurjchem-208	435	59	materials	material	NOUN
eurjchem-208	435	60	4b	4b	PROPN
eurjchem-208	435	61	and	and	CCONJ
eurjchem-208	435	62	18	18	NUM
eurjchem-208	435	63	.	.	PUNCT
eurjchem-208	435	64	acknowledgement	acknowledgement	NOUN
eurjchem-208	435	65	we	we	PRON
eurjchem-208	435	66	thank	thank	VERB
eurjchem-208	435	67	department	department	PROPN
eurjchem-208	435	68	of	of	ADP
eurjchem-208	435	69	microbiology	microbiology	NOUN
eurjchem-208	435	70	,	,	PUNCT
eurjchem-208	435	71	faculty	faculty	NOUN
eurjchem-208	435	72	of	of	ADP
eurjchem-208	435	73	agriculture	agriculture	NOUN
eurjchem-208	435	74	,	,	PUNCT
eurjchem-208	435	75	al‐azhar	al‐azhar	PROPN
eurjchem-208	435	76	university	university	PROPN
eurjchem-208	435	77	for	for	ADP
eurjchem-208	435	78	girls	girl	NOUN
eurjchem-208	435	79	,	,	PUNCT
eurjchem-208	435	80	nasr‐city	nasr‐city	PROPN
eurjchem-208	435	81	,	,	PUNCT
eurjchem-208	435	82	cairo	cairo	PROPN
eurjchem-208	435	83	,	,	PUNCT
eurjchem-208	435	84	egypt	egypt	PROPN
eurjchem-208	435	85	,	,	PUNCT
eurjchem-208	435	86	for	for	ADP
eurjchem-208	435	87	evaluation	evaluation	NOUN
eurjchem-208	435	88	of	of	ADP
eurjchem-208	435	89	antimicrobial	antimicrobial	ADJ
eurjchem-208	435	90	activities	activity	NOUN
eurjchem-208	435	91	for	for	ADP
eurjchem-208	435	92	the	the	DET
eurjchem-208	435	93	prepared	prepare	VERB
eurjchem-208	435	94	compounds	compound	NOUN
eurjchem-208	435	95	.	.	PUNCT
eurjchem-208	436	1	0	0	NUM
eurjchem-208	436	2	5	5	NUM
eurjchem-208	436	3	10	10	NUM
eurjchem-208	436	4	15	15	NUM
eurjchem-208	436	5	20	20	NUM
eurjchem-208	436	6	25	25	NUM
eurjchem-208	436	7	30	30	NUM
eurjchem-208	436	8	35	35	NUM
eurjchem-208	436	9	40	40	NUM
eurjchem-208	436	10	s.	s.	PROPN
eurjchem-208	436	11	aureus	aureus	PROPN
eurjchem-208	436	12	s.	s.	PROPN
eurjchem-208	436	13	pyogenes	pyogenes	PROPN
eurjchem-208	436	14	p.	p.	PROPN
eurjchem-208	436	15	phaseolicola	phaseolicola	PROPN
eurjchem-208	437	1	p.	p.	NOUN
eurjchem-208	437	2	fluorescens	fluorescens	PROPN
eurjchem-208	438	1	f.	f.	PROPN
eurjchem-208	438	2	oxysporum	oxysporum	PROPN
eurjchem-208	438	3	a.	a.	PROPN
eurjchem-208	438	4	fumigatus	fumigatus	NOUN
eurjchem-208	438	5	microbial	microbial	ADJ
eurjchem-208	438	6	strains	strain	NOUN
eurjchem-208	438	7	in	in	ADP
eurjchem-208	438	8	h	h	NOUN
eurjchem-208	438	9	ib	ib	NOUN
eurjchem-208	438	10	it	it	PRON
eurjchem-208	438	11	io	io	PROPN
eurjchem-208	438	12	n	n	ADV
eurjchem-208	438	13	z	z	NOUN
eurjchem-208	438	14	o	o	NOUN
eurjchem-208	439	1	n	n	X
eurjchem-208	439	2	e	e	X
eurjchem-208	439	3	s	s	X
eurjchem-208	439	4	(	(	PUNCT
eurjchem-208	439	5	m	m	VERB
eurjchem-208	439	6	m	m	VERB
eurjchem-208	439	7	)	)	PUNCT
eurjchem-208	439	8	a	a	DET
eurjchem-208	439	9	t	t	NOUN
eurjchem-208	439	10	2	2	NUM
eurjchem-208	439	11	m	m	NOUN
eurjchem-208	439	12	g	g	NOUN
eurjchem-208	439	13	/m	/m	PUNCT
eurjchem-208	439	14	l	l	NOUN
eurjchem-208	439	15	compound	compound	NOUN
eurjchem-208	439	16	11	11	NUM
eurjchem-208	439	17	compound	compound	NOUN
eurjchem-208	439	18	16	16	NUM
eurjchem-208	439	19	compound	compound	NOUN
eurjchem-208	439	20	22	22	NUM
eurjchem-208	439	21	figure	figure	NOUN
eurjchem-208	439	22	4	4	NUM
eurjchem-208	439	23	.	.	PUNCT
eurjchem-208	439	24	relationship	relationship	NOUN
eurjchem-208	439	25	between	between	ADP
eurjchem-208	439	26	inhibition	inhibition	NOUN
eurjchem-208	439	27	zones	zone	NOUN
eurjchem-208	439	28	at	at	ADP
eurjchem-208	439	29	2	2	NUM
eurjchem-208	439	30	mg	mg	NUM
eurjchem-208	439	31	/	/	SYM
eurjchem-208	439	32	ml	ml	NOUN
eurjchem-208	439	33	and	and	CCONJ
eurjchem-208	439	34	microbial	microbial	ADJ
eurjchem-208	439	35	strains	strain	NOUN
eurjchem-208	439	36	for	for	ADP
eurjchem-208	439	37	compounds	compound	NOUN
eurjchem-208	439	38	11	11	NUM
eurjchem-208	439	39	,	,	PUNCT
eurjchem-208	439	40	16	16	NUM
eurjchem-208	439	41	and	and	CCONJ
eurjchem-208	439	42	22	22	NUM
eurjchem-208	439	43	(	(	PUNCT
eurjchem-208	439	44	including	include	VERB
eurjchem-208	439	45	extra	extra	ADJ
eurjchem-208	439	46	phosphorus	phosphorus	NOUN
eurjchem-208	439	47	atoms	atom	NOUN
eurjchem-208	439	48	in	in	ADP
eurjchem-208	439	49	shape	shape	NOUN
eurjchem-208	439	50	acyclic	acyclic	ADJ
eurjchem-208	439	51	‐aminophosphonate	‐aminophosphonate	NOUN
eurjchem-208	439	52	,	,	PUNCT
eurjchem-208	439	53	ethyl	ethyl	PROPN
eurjchem-208	439	54	phosphonate	phosphonate	NOUN
eurjchem-208	439	55	and	and	CCONJ
eurjchem-208	439	56	cyclic	cyclic	ADJ
eurjchem-208	439	57	‐amino‐	‐amino‐	PROPN
eurjchem-208	439	58	phosphonate	phosphonate	ADJ
eurjchem-208	439	59	moieties	moiety	NOUN
eurjchem-208	439	60	,	,	PUNCT
eurjchem-208	439	61	respectively	respectively	ADV
eurjchem-208	439	62	)	)	PUNCT
eurjchem-208	439	63	which	which	PRON
eurjchem-208	439	64	showed	show	VERB
eurjchem-208	439	65	good	good	ADJ
eurjchem-208	439	66	inhibitions	inhibition	NOUN
eurjchem-208	439	67	against	against	ADP
eurjchem-208	439	68	all	all	DET
eurjchem-208	439	69	microbial	microbial	ADJ
eurjchem-208	439	70	strains	strain	NOUN
eurjchem-208	439	71	.	.	PUNCT
eurjchem-208	440	1	compound	compound	NOUN
eurjchem-208	440	2	22	22	NUM
eurjchem-208	440	3	is	be	AUX
eurjchem-208	440	4	the	the	DET
eurjchem-208	440	5	highest	high	ADJ
eurjchem-208	440	6	one	one	NOUN
eurjchem-208	440	7	because	because	SCONJ
eurjchem-208	440	8	it	it	PRON
eurjchem-208	440	9	contains	contain	VERB
eurjchem-208	440	10	cyclic	cyclic	ADJ
eurjchem-208	440	11	α‐aminophosphonate	α‐aminophosphonate	PUNCT
eurjchem-208	440	12	moiety	moiety	NOUN
eurjchem-208	440	13	in	in	ADP
eurjchem-208	440	14	addition	addition	NOUN
eurjchem-208	440	15	to	to	ADP
eurjchem-208	440	16	sulfur	sulfur	NOUN
eurjchem-208	440	17	element	element	NOUN
eurjchem-208	440	18	which	which	PRON
eurjchem-208	440	19	revealed	reveal	VERB
eurjchem-208	440	20	that	that	SCONJ
eurjchem-208	440	21	the	the	DET
eurjchem-208	440	22	presence	presence	NOUN
eurjchem-208	440	23	of	of	ADP
eurjchem-208	440	24	phosphorus	phosphorus	NOUN
eurjchem-208	440	25	and	and	CCONJ
eurjchem-208	440	26	sulfur	sulfur	NOUN
eurjchem-208	440	27	in	in	ADP
eurjchem-208	440	28	one	one	NUM
eurjchem-208	440	29	compound	compound	NOUN
eurjchem-208	440	30	enhance	enhance	VERB
eurjchem-208	440	31	very	very	ADV
eurjchem-208	440	32	clear	clear	ADJ
eurjchem-208	440	33	increase	increase	NOUN
eurjchem-208	440	34	in	in	ADP
eurjchem-208	440	35	activity	activity	NOUN
eurjchem-208	440	36	.	.	PUNCT
eurjchem-208	441	1	references	reference	NOUN
eurjchem-208	441	2	[	[	X
eurjchem-208	441	3	1	1	NUM
eurjchem-208	441	4	]	]	PUNCT
eurjchem-208	441	5	.	.	PUNCT
eurjchem-208	442	1	mitchell	mitchell	PROPN
eurjchem-208	442	2	,	,	PUNCT
eurjchem-208	442	3	r.	r.	PROPN
eurjchem-208	442	4	e.	e.	PROPN
eurjchem-208	442	5	;	;	PUNCT
eurjchem-208	442	6	greenwood	greenwood	PROPN
eurjchem-208	442	7	,	,	PUNCT
eurjchem-208	442	8	d.	d.	PROPN
eurjchem-208	442	9	r.	r.	PROPN
eurjchem-208	442	10	;	;	PUNCT
eurjchem-208	442	11	sarojini	sarojini	PROPN
eurjchem-208	442	12	,	,	PUNCT
eurjchem-208	442	13	v.	v.	ADP
eurjchem-208	442	14	phytochemistry	phytochemistry	PROPN
eurjchem-208	442	15	2008	2008	NUM
eurjchem-208	442	16	,	,	PUNCT
eurjchem-208	442	17	69	69	NUM
eurjchem-208	442	18	,	,	PUNCT
eurjchem-208	442	19	2704‐2707	2704‐2707	NUM
eurjchem-208	442	20	.	.	PUNCT
eurjchem-208	443	1	[	[	X
eurjchem-208	443	2	2	2	NUM
eurjchem-208	443	3	]	]	PUNCT
eurjchem-208	443	4	.	.	PUNCT
eurjchem-208	443	5	abdel‐hafez	abdel‐hafez	PROPN
eurjchem-208	443	6	,	,	PUNCT
eurjchem-208	443	7	e.	e.	PROPN
eurjchem-208	443	8	m.	m.	PROPN
eurjchem-208	443	9	n.	n.	PROPN
eurjchem-208	443	10	;	;	PUNCT
eurjchem-208	443	11	abuo‐rahma	abuo‐rahma	ADV
eurjchem-208	443	12	,	,	PUNCT
eurjchem-208	443	13	g.	g.	PROPN
eurjchem-208	443	14	a.	a.	PROPN
eurjchem-208	443	15	a.	a.	PROPN
eurjchem-208	443	16	;	;	PUNCT
eurjchem-208	443	17	abdel‐aziz	abdel‐aziz	NOUN
eurjchem-208	443	18	,	,	PUNCT
eurjchem-208	443	19	m.	m.	NOUN
eurjchem-208	443	20	;	;	PUNCT
eurjchem-208	443	21	radwan	radwan	NOUN
eurjchem-208	443	22	,	,	PUNCT
eurjchem-208	443	23	m.	m.	PROPN
eurjchem-208	443	24	f.	f.	PROPN
eurjchem-208	443	25	;	;	PUNCT
eurjchem-208	443	26	farag	farag	PROPN
eurjchem-208	443	27	,	,	PUNCT
eurjchem-208	443	28	h.	h.	PROPN
eurjchem-208	443	29	h.	h.	PROPN
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eurjchem-208	443	31	.	.	PUNCT
eurjchem-208	444	1	med	med	PROPN
eurjchem-208	444	2	.	.	PUNCT
eurjchem-208	444	3	chem	chem	PROPN
eurjchem-208	444	4	.	.	PUNCT
eurjchem-208	445	1	2009	2009	NUM
eurjchem-208	445	2	,	,	PUNCT
eurjchem-208	445	3	17	17	NUM
eurjchem-208	445	4	,	,	PUNCT
eurjchem-208	445	5	3829‐3837	3829‐3837	NUM
eurjchem-208	445	6	.	.	PUNCT
eurjchem-208	446	1	[	[	X
eurjchem-208	446	2	3	3	NUM
eurjchem-208	446	3	]	]	PUNCT
eurjchem-208	446	4	.	.	PUNCT
eurjchem-208	447	1	ali	ali	PROPN
eurjchem-208	447	2	,	,	PUNCT
eurjchem-208	447	3	t.	t.	PROPN
eurjchem-208	447	4	e.	e.	PROPN
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eurjchem-208	448	1	j.	j.	PROPN
eurjchem-208	448	2	med	med	PROPN
eurjchem-208	448	3	.	.	PROPN
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eurjchem-208	448	5	.	.	PUNCT
eurjchem-208	449	1	2009	2009	NUM
eurjchem-208	449	2	,	,	PUNCT
eurjchem-208	449	3	44	44	NUM
eurjchem-208	449	4	,	,	PUNCT
eurjchem-208	449	5	4385‐4392	4385‐4392	NUM
eurjchem-208	449	6	.	.	PUNCT
eurjchem-208	450	1	[	[	X
eurjchem-208	450	2	4	4	NUM
eurjchem-208	450	3	]	]	PUNCT
eurjchem-208	450	4	.	.	PUNCT
eurjchem-208	451	1	rai	rai	PROPN
eurjchem-208	451	2	,	,	PUNCT
eurjchem-208	451	3	n.	n.	PROPN
eurjchem-208	451	4	s.	s.	PROPN
eurjchem-208	451	5	;	;	PUNCT
eurjchem-208	451	6	kalluraya	kalluraya	PROPN
eurjchem-208	451	7	,	,	PUNCT
eurjchem-208	451	8	b.	b.	PROPN
eurjchem-208	451	9	;	;	PUNCT
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eurjchem-208	451	11	,	,	PUNCT
eurjchem-208	451	12	b.	b.	PROPN
eurjchem-208	451	13	;	;	PUNCT
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eurjchem-208	451	15	,	,	PUNCT
eurjchem-208	451	16	s.	s.	PROPN
eurjchem-208	451	17	;	;	PUNCT
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eurjchem-208	451	19	,	,	PUNCT
eurjchem-208	451	20	v.	v.	PROPN
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eurjchem-208	452	1	j.	j.	PROPN
eurjchem-208	452	2	med	med	PROPN
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eurjchem-208	453	2	,	,	PUNCT
eurjchem-208	453	3	43	43	NUM
eurjchem-208	453	4	,	,	PUNCT
eurjchem-208	453	5	1715‐1720	1715‐1720	NUM
eurjchem-208	453	6	.	.	PUNCT
eurjchem-208	454	1	[	[	X
eurjchem-208	454	2	5	5	NUM
eurjchem-208	454	3	]	]	PUNCT
eurjchem-208	454	4	.	.	PUNCT
eurjchem-208	454	5	witschel	witschel	PROPN
eurjchem-208	454	6	,	,	PUNCT
eurjchem-208	454	7	m.	m.	NOUN
eurjchem-208	454	8	bioorg	bioorg	PROPN
eurjchem-208	454	9	.	.	PUNCT
eurjchem-208	455	1	med	med	PROPN
eurjchem-208	455	2	.	.	PUNCT
eurjchem-208	455	3	chem	chem	PROPN
eurjchem-208	455	4	.	.	PUNCT
eurjchem-208	456	1	2009	2009	NUM
eurjchem-208	456	2	,	,	PUNCT
eurjchem-208	456	3	17	17	NUM
eurjchem-208	456	4	,	,	PUNCT
eurjchem-208	456	5	4221‐4229	4221‐4229	NUM
eurjchem-208	456	6	.	.	PUNCT
eurjchem-208	457	1	[	[	X
eurjchem-208	457	2	6	6	NUM
eurjchem-208	457	3	]	]	PUNCT
eurjchem-208	457	4	.	.	PUNCT
eurjchem-208	458	1	lahm	lahm	PROPN
eurjchem-208	458	2	,	,	PUNCT
eurjchem-208	458	3	g.	g.	PROPN
eurjchem-208	458	4	p.	p.	PROPN
eurjchem-208	458	5	;	;	PUNCT
eurjchem-208	458	6	stevenson	stevenson	PROPN
eurjchem-208	458	7	,	,	PUNCT
eurjchem-208	458	8	t.	t.	NOUN
eurjchem-208	458	9	m.	m.	NOUN
eurjchem-208	458	10	;	;	PUNCT
eurjchem-208	458	11	selby	selby	PROPN
eurjchem-208	458	12	,	,	PUNCT
eurjchem-208	458	13	t.	t.	PROPN
eurjchem-208	458	14	p.	p.	PROPN
eurjchem-208	458	15	;	;	PUNCT
eurjchem-208	458	16	freudenberger	freudenberger	PROPN
eurjchem-208	458	17	,	,	PUNCT
eurjchem-208	458	18	j.	j.	PROPN
eurjchem-208	458	19	h.	h.	PROPN
eurjchem-208	458	20	;	;	PUNCT
eurjchem-208	458	21	cordova	cordova	PROPN
eurjchem-208	458	22	,	,	PUNCT
eurjchem-208	458	23	d.	d.	PROPN
eurjchem-208	458	24	;	;	PUNCT
eurjchem-208	458	25	flexner	flexner	NOUN
eurjchem-208	458	26	,	,	PUNCT
eurjchem-208	458	27	l.	l.	PROPN
eurjchem-208	458	28	;	;	PUNCT
eurjchem-208	458	29	bellin	bellin	PROPN
eurjchem-208	458	30	,	,	PUNCT
eurjchem-208	458	31	c.	c.	PROPN
eurjchem-208	458	32	a.	a.	PROPN
eurjchem-208	458	33	;	;	PUNCT
eurjchem-208	458	34	dubas	dubas	PROPN
eurjchem-208	458	35	,	,	PUNCT
eurjchem-208	458	36	c.	c.	PROPN
eurjchem-208	458	37	m.	m.	NOUN
eurjchem-208	458	38	;	;	PUNCT
eurjchem-208	458	39	smith	smith	PROPN
eurjchem-208	458	40	,	,	PUNCT
eurjchem-208	458	41	b.	b.	PROPN
eurjchem-208	458	42	k.	k.	PROPN
eurjchem-208	458	43	;	;	PUNCT
eurjchem-208	458	44	hughes	hughes	PROPN
eurjchem-208	458	45	,	,	PUNCT
eurjchem-208	458	46	k.	k.	PROPN
eurjchem-208	458	47	a.	a.	PROPN
eurjchem-208	458	48	;	;	PUNCT
eurjchem-208	458	49	hollingshaus	hollingshaus	PROPN
eurjchem-208	458	50	,	,	PUNCT
eurjchem-208	458	51	j.	j.	PROPN
eurjchem-208	458	52	g.	g.	PROPN
eurjchem-208	458	53	;	;	PUNCT
eurjchem-208	458	54	clark	clark	PROPN
eurjchem-208	458	55	,	,	PUNCT
eurjchem-208	458	56	c.	c.	PROPN
eurjchem-208	458	57	e.	e.	PROPN
eurjchem-208	458	58	;	;	PUNCT
eurjchem-208	458	59	benner	benner	PROPN
eurjchem-208	458	60	,	,	PUNCT
eurjchem-208	458	61	e.	e.	PROPN
eurjchem-208	458	62	a.	a.	PROPN
eurjchem-208	458	63	bioorg	bioorg	PROPN
eurjchem-208	458	64	.	.	PUNCT
eurjchem-208	459	1	med	med	PROPN
eurjchem-208	459	2	.	.	PROPN
eurjchem-208	459	3	chem	chem	PROPN
eurjchem-208	459	4	.	.	PUNCT
eurjchem-208	460	1	lett	lett	PROPN
eurjchem-208	460	2	.	.	PUNCT
eurjchem-208	461	1	2007	2007	NUM
eurjchem-208	461	2	,	,	PUNCT
eurjchem-208	461	3	17	17	NUM
eurjchem-208	461	4	,	,	PUNCT
eurjchem-208	461	5	6274‐6279	6274‐6279	NUM
eurjchem-208	461	6	.	.	PUNCT
eurjchem-208	462	1	[	[	X
eurjchem-208	462	2	7	7	NUM
eurjchem-208	462	3	]	]	PUNCT
eurjchem-208	462	4	.	.	PUNCT
eurjchem-208	463	1	kopp	kopp	PROPN
eurjchem-208	463	2	,	,	PUNCT
eurjchem-208	463	3	m.	m.	NOUN
eurjchem-208	463	4	;	;	PUNCT
eurjchem-208	463	5	lancelot	lancelot	PROPN
eurjchem-208	463	6	,	,	PUNCT
eurjchem-208	463	7	j.	j.	PROPN
eurjchem-208	463	8	c.	c.	PROPN
eurjchem-208	463	9	;	;	PUNCT
eurjchem-208	463	10	dallemagne	dallemagne	PROPN
eurjchem-208	463	11	,	,	PUNCT
eurjchem-208	463	12	p.	p.	NOUN
eurjchem-208	463	13	;	;	PUNCT
eurjchem-208	463	14	rault	rault	NOUN
eurjchem-208	463	15	,	,	PUNCT
eurjchem-208	463	16	s.	s.	PROPN
eurjchem-208	463	17	j.	j.	PROPN
eurjchem-208	463	18	heterocycl	heterocycl	PROPN
eurjchem-208	463	19	.	.	PUNCT
eurjchem-208	464	1	chem	chem	PROPN
eurjchem-208	464	2	.	.	PUNCT
eurjchem-208	465	1	2001	2001	NUM
eurjchem-208	465	2	,	,	PUNCT
eurjchem-208	465	3	38	38	NUM
eurjchem-208	465	4	,	,	PUNCT
eurjchem-208	465	5	1045‐1050	1045‐1050	NUM
eurjchem-208	465	6	.	.	PUNCT
eurjchem-208	466	1	[	[	X
eurjchem-208	466	2	8	8	NUM
eurjchem-208	466	3	]	]	SYM
eurjchem-208	466	4	.	.	PUNCT
eurjchem-208	466	5	colliot	colliot	PROPN
eurjchem-208	466	6	,	,	PUNCT
eurjchem-208	466	7	f.	f.	PROPN
eurjchem-208	466	8	;	;	PUNCT
eurjchem-208	466	9	kukorowski	kukorowski	PROPN
eurjchem-208	466	10	,	,	PUNCT
eurjchem-208	466	11	k.	k.	PROPN
eurjchem-208	466	12	a.	a.	PROPN
eurjchem-208	466	13	;	;	PUNCT
eurjchem-208	466	14	hawkins	hawkins	PROPN
eurjchem-208	466	15	,	,	PUNCT
eurjchem-208	466	16	d.	d.	PROPN
eurjchem-208	466	17	w.	w.	PROPN
eurjchem-208	466	18	;	;	PUNCT
eurjchem-208	466	19	roberts	roberts	PROPN
eurjchem-208	466	20	,	,	PUNCT
eurjchem-208	466	21	d.	d.	PROPN
eurjchem-208	466	22	a.	a.	PROPN
eurjchem-208	466	23	brighton	brighton	PROPN
eurjchem-208	466	24	crop	crop	PROPN
eurjchem-208	466	25	prot	prot	NOUN
eurjchem-208	466	26	.	.	PUNCT
eurjchem-208	467	1	conf	conf	NOUN
eurjchem-208	467	2	.	.	PUNCT
eurjchem-208	468	1	pests	pest	NOUN
eurjchem-208	468	2	dis	dis	PROPN
eurjchem-208	468	3	.	.	PUNCT
eurjchem-208	468	4	1992	1992	NUM
eurjchem-208	468	5	,	,	PUNCT
eurjchem-208	468	6	1	1	NUM
eurjchem-208	468	7	,	,	PUNCT
eurjchem-208	468	8	29‐34	29‐34	ADJ
eurjchem-208	468	9	.	.	PUNCT
eurjchem-208	469	1	[	[	X
eurjchem-208	469	2	9	9	NUM
eurjchem-208	469	3	]	]	PUNCT
eurjchem-208	469	4	.	.	PUNCT
eurjchem-208	470	1	miura	miura	PROPN
eurjchem-208	470	2	,	,	PUNCT
eurjchem-208	470	3	y.	y.	PROPN
eurjchem-208	470	4	;	;	PUNCT
eurjchem-208	470	5	ohnishi	ohnishi	PROPN
eurjchem-208	470	6	,	,	PUNCT
eurjchem-208	470	7	m.	m.	NOUN
eurjchem-208	470	8	;	;	PUNCT
eurjchem-208	470	9	mabuchi	mabuchi	PROPN
eurjchem-208	470	10	,	,	PUNCT
eurjchem-208	470	11	t.	t.	PROPN
eurjchem-208	470	12	;	;	PUNCT
eurjchem-208	470	13	yanai	yanai	PROPN
eurjchem-208	470	14	,	,	PUNCT
eurjchem-208	470	15	i.	i.	PROPN
eurjchem-208	470	16	brighton	brighton	PROPN
eurjchem-208	470	17	crop	crop	PROPN
eurjchem-208	470	18	prot	prot	NOUN
eurjchem-208	470	19	.	.	PUNCT
eurjchem-208	471	1	conf	conf	NOUN
eurjchem-208	471	2	.	.	PUNCT
eurjchem-208	472	1	weeds	weed	NOUN
eurjchem-208	472	2	1993	1993	NUM
eurjchem-208	472	3	,	,	PUNCT
eurjchem-208	472	4	1	1	NUM
eurjchem-208	472	5	,	,	PUNCT
eurjchem-208	472	6	35‐41	35‐41	NUM
eurjchem-208	472	7	.	.	PUNCT
eurjchem-208	473	1	[	[	X
eurjchem-208	473	2	10	10	NUM
eurjchem-208	473	3	]	]	PUNCT
eurjchem-208	473	4	.	.	PUNCT
eurjchem-208	474	1	konotsune	konotsune	PROPN
eurjchem-208	474	2	,	,	PUNCT
eurjchem-208	474	3	t.	t.	PROPN
eurjchem-208	474	4	;	;	PUNCT
eurjchem-208	474	5	kawakubo	kawakubo	PROPN
eurjchem-208	474	6	,	,	PUNCT
eurjchem-208	474	7	k.	k.	PROPN
eurjchem-208	474	8	;	;	PUNCT
eurjchem-208	474	9	honma	honma	PROPN
eurjchem-208	474	10	,	,	PUNCT
eurjchem-208	474	11	t.	t.	PROPN
eurjchem-208	474	12	jap	jap	PROPN
eurjchem-208	474	13	.	.	PUNCT
eurjchem-208	475	1	pat	pat	PROPN
eurjchem-208	475	2	.	.	PROPN
eurjchem-208	475	3	1980	1980	NUM
eurjchem-208	475	4	,	,	PUNCT
eurjchem-208	475	5	8035035	8035035	NUM
eurjchem-208	475	6	;	;	PUNCT
eurjchem-208	475	7	chem	chem	NOUN
eurjchem-208	475	8	.	.	PUNCT
eurjchem-208	476	1	abstr	abstr	PROPN
eurjchem-208	476	2	.	.	PUNCT
eurjchem-208	477	1	1980	1980	NUM
eurjchem-208	477	2	,	,	PUNCT
eurjchem-208	477	3	93	93	NUM
eurjchem-208	477	4	,	,	PUNCT
eurjchem-208	477	5	20750	20750	NUM
eurjchem-208	477	6	.	.	PUNCT
eurjchem-208	478	1	[	[	X
eurjchem-208	478	2	11	11	NUM
eurjchem-208	478	3	]	]	PUNCT
eurjchem-208	478	4	.	.	PUNCT
eurjchem-208	478	5	sengupta	sengupta	NOUN
eurjchem-208	478	6	,	,	PUNCT
eurjchem-208	478	7	s.	s.	PROPN
eurjchem-208	478	8	k.	k.	PROPN
eurjchem-208	478	9	;	;	PUNCT
eurjchem-208	478	10	pandey	pandey	PROPN
eurjchem-208	478	11	,	,	PUNCT
eurjchem-208	478	12	o.	o.	PROPN
eurjchem-208	478	13	p.	p.	PROPN
eurjchem-208	478	14	;	;	PUNCT
eurjchem-208	478	15	rao	rao	PROPN
eurjchem-208	478	16	,	,	PUNCT
eurjchem-208	478	17	g.	g.	PROPN
eurjchem-208	478	18	p.	p.	PROPN
eurjchem-208	478	19	;	;	PUNCT
eurjchem-208	478	20	dwivedi	dwivedi	PROPN
eurjchem-208	478	21	,	,	PUNCT
eurjchem-208	478	22	a.	a.	NOUN
eurjchem-208	478	23	;	;	PUNCT
eurjchem-208	478	24	singh	singh	PROPN
eurjchem-208	478	25	,	,	PUNCT
eurjchem-208	478	26	p.	p.	NOUN
eurjchem-208	478	27	phosphorus	phosphorus	NOUN
eurjchem-208	478	28	,	,	PUNCT
eurjchem-208	478	29	sulfur	sulfur	NOUN
eurjchem-208	478	30	silicon	silicon	NOUN
eurjchem-208	478	31	relat	relat	PROPN
eurjchem-208	478	32	.	.	PUNCT
eurjchem-208	479	1	elem	elem	NOUN
eurjchem-208	479	2	.	.	PUNCT
eurjchem-208	480	1	2003	2003	NUM
eurjchem-208	480	2	,	,	PUNCT
eurjchem-208	480	3	178	178	NUM
eurjchem-208	480	4	,	,	PUNCT
eurjchem-208	480	5	839‐849	839‐849	NUM
eurjchem-208	480	6	.	.	PUNCT
eurjchem-208	481	1	[	[	X
eurjchem-208	481	2	12	12	NUM
eurjchem-208	481	3	]	]	PUNCT
eurjchem-208	481	4	.	.	PUNCT
eurjchem-208	482	1	sengupta	sengupta	NOUN
eurjchem-208	482	2	,	,	PUNCT
eurjchem-208	482	3	s.	s.	PROPN
eurjchem-208	482	4	k.	k.	PROPN
eurjchem-208	482	5	;	;	PUNCT
eurjchem-208	482	6	pandey	pandey	PROPN
eurjchem-208	482	7	,	,	PUNCT
eurjchem-208	482	8	o.	o.	PROPN
eurjchem-208	482	9	p.	p.	PROPN
eurjchem-208	482	10	;	;	PUNCT
eurjchem-208	482	11	rao	rao	PROPN
eurjchem-208	482	12	,	,	PUNCT
eurjchem-208	482	13	g.	g.	PROPN
eurjchem-208	482	14	p.	p.	PROPN
eurjchem-208	482	15	;	;	PUNCT
eurjchem-208	482	16	singh	singh	PROPN
eurjchem-208	482	17	,	,	PUNCT
eurjchem-208	482	18	p.	p.	PROPN
eurjchem-208	482	19	metal‐based	metal‐base	VERB
eurjchem-208	482	20	drugs	drug	NOUN
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eurjchem-208	482	22	,	,	PUNCT
eurjchem-208	482	23	8	8	NUM
eurjchem-208	482	24	,	,	PUNCT
eurjchem-208	482	25	293‐302	293‐302	NUM
eurjchem-208	482	26	.	.	PUNCT
eurjchem-208	483	1	[	[	X
eurjchem-208	483	2	13	13	NUM
eurjchem-208	483	3	]	]	SYM
eurjchem-208	483	4	.	.	PUNCT
eurjchem-208	484	1	ali	ali	PROPN
eurjchem-208	484	2	,	,	PUNCT
eurjchem-208	484	3	t.	t.	PROPN
eurjchem-208	484	4	e.	e.	PROPN
eurjchem-208	484	5	;	;	PUNCT
eurjchem-208	484	6	abdel‐rahman	abdel‐rahman	NOUN
eurjchem-208	484	7	,	,	PUNCT
eurjchem-208	484	8	r.	r.	PROPN
eurjchem-208	484	9	m.	m.	PROPN
eurjchem-208	484	10	;	;	PUNCT
eurjchem-208	484	11	hanafy	hanafy	PROPN
eurjchem-208	484	12	,	,	PUNCT
eurjchem-208	484	13	f.	f.	PROPN
eurjchem-208	484	14	i.	i.	PROPN
eurjchem-208	484	15	;	;	PUNCT
eurjchem-208	484	16	el‐edfawy	el‐edfawy	PROPN
eurjchem-208	484	17	,	,	PUNCT
eurjchem-208	484	18	s.	s.	PROPN
eurjchem-208	484	19	m.	m.	NOUN
eurjchem-208	484	20	phosphorus	phosphorus	PROPN
eurjchem-208	484	21	,	,	PUNCT
eurjchem-208	484	22	sulfur	sulfur	NOUN
eurjchem-208	484	23	silicon	silicon	NOUN
eurjchem-208	484	24	relat	relat	PROPN
eurjchem-208	484	25	.	.	PUNCT
eurjchem-208	485	1	elem	elem	NOUN
eurjchem-208	485	2	.	.	PUNCT
eurjchem-208	486	1	2008	2008	NUM
eurjchem-208	486	2	,	,	PUNCT
eurjchem-208	486	3	183	183	NUM
eurjchem-208	486	4	,	,	PUNCT
eurjchem-208	486	5	2565‐2577	2565‐2577	NUM
eurjchem-208	486	6	.	.	PUNCT
eurjchem-208	487	1	[	[	X
eurjchem-208	487	2	14	14	NUM
eurjchem-208	487	3	]	]	PUNCT
eurjchem-208	487	4	.	.	PUNCT
eurjchem-208	488	1	pareek	pareek	PROPN
eurjchem-208	488	2	,	,	PUNCT
eurjchem-208	488	3	s.	s.	PROPN
eurjchem-208	488	4	;	;	PUNCT
eurjchem-208	488	5	vyas	vyas	PROPN
eurjchem-208	488	6	,	,	PUNCT
eurjchem-208	488	7	s.	s.	PROPN
eurjchem-208	488	8	;	;	PUNCT
eurjchem-208	488	9	seth	seth	PROPN
eurjchem-208	488	10	,	,	PUNCT
eurjchem-208	488	11	g.	g.	PROPN
eurjchem-208	488	12	;	;	PUNCT
eurjchem-208	488	13	vyas	vyas	PROPN
eurjchem-208	488	14	,	,	PUNCT
eurjchem-208	488	15	p.	p.	PROPN
eurjchem-208	488	16	c.	c.	PROPN
eurjchem-208	488	17	heteroatom	heteroatom	PROPN
eurjchem-208	488	18	chem	chem	PROPN
eurjchem-208	488	19	.	.	PUNCT
eurjchem-208	489	1	2009	2009	NUM
eurjchem-208	489	2	,	,	PUNCT
eurjchem-208	489	3	20	20	NUM
eurjchem-208	489	4	,	,	PUNCT
eurjchem-208	489	5	246‐249	246‐249	NUM
eurjchem-208	489	6	.	.	PUNCT
eurjchem-208	490	1	[	[	X
eurjchem-208	490	2	15	15	NUM
eurjchem-208	490	3	]	]	SYM
eurjchem-208	490	4	.	.	PUNCT
eurjchem-208	491	1	ali	ali	PROPN
eurjchem-208	491	2	,	,	PUNCT
eurjchem-208	491	3	t.	t.	PROPN
eurjchem-208	491	4	e.	e.	PROPN
eurjchem-208	491	5	eur	eur	PROPN
eurjchem-208	491	6	.	.	PUNCT
eurjchem-208	492	1	j.	j.	PROPN
eurjchem-208	492	2	med	med	PROPN
eurjchem-208	492	3	.	.	PROPN
eurjchem-208	492	4	chem	chem	PROPN
eurjchem-208	492	5	.	.	PUNCT
eurjchem-208	493	1	2009	2009	NUM
eurjchem-208	493	2	,	,	PUNCT
eurjchem-208	493	3	44	44	NUM
eurjchem-208	493	4	,	,	PUNCT
eurjchem-208	493	5	4539‐4546	4539‐4546	NUM
eurjchem-208	493	6	.	.	PUNCT
eurjchem-208	494	1	[	[	X
eurjchem-208	494	2	16	16	NUM
eurjchem-208	494	3	]	]	PUNCT
eurjchem-208	494	4	.	.	PUNCT
eurjchem-208	495	1	fest	f	ADJ
eurjchem-208	495	2	,	,	PUNCT
eurjchem-208	495	3	c.	c.	PROPN
eurjchem-208	495	4	;	;	PUNCT
eurjchem-208	495	5	schmidt	schmidt	PROPN
eurjchem-208	495	6	,	,	PUNCT
eurjchem-208	495	7	k.	k.	PROPN
eurjchem-208	495	8	j.	j.	PROPN
eurjchem-208	495	9	chemistry	chemistry	PROPN
eurjchem-208	495	10	of	of	ADP
eurjchem-208	495	11	organophosphorus	organophosphorus	NOUN
eurjchem-208	495	12	compounds	compound	NOUN
eurjchem-208	495	13	;	;	PUNCT
eurjchem-208	495	14	springer‐verlag	springer‐verlag	PROPN
eurjchem-208	495	15	:	:	PUNCT
eurjchem-208	495	16	berlin	berlin	PROPN
eurjchem-208	495	17	,	,	PUNCT
eurjchem-208	495	18	1973	1973	NUM
eurjchem-208	495	19	.	.	PUNCT
eurjchem-208	496	1	[	[	X
eurjchem-208	496	2	17	17	NUM
eurjchem-208	496	3	]	]	PUNCT
eurjchem-208	496	4	.	.	PUNCT
eurjchem-208	497	1	troev	troev	PROPN
eurjchem-208	497	2	,	,	PUNCT
eurjchem-208	497	3	k.	k.	PROPN
eurjchem-208	497	4	d.	d.	PROPN
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eurjchem-208	497	10	;	;	PUNCT
eurjchem-208	497	11	elsevier	elsevier	NOUN
eurjchem-208	497	12	,	,	PUNCT
eurjchem-208	497	13	amsterdam	amsterdam	PROPN
eurjchem-208	497	14	,	,	PUNCT
eurjchem-208	497	15	2006	2006	NUM
eurjchem-208	497	16	,	,	PUNCT
eurjchem-208	497	17	pp	pp	ADV
eurjchem-208	497	18	.	.	PUNCT
eurjchem-208	498	1	253‐261	253‐261	NUM
eurjchem-208	498	2	.	.	PUNCT
eurjchem-208	499	1	[	[	X
eurjchem-208	499	2	18	18	NUM
eurjchem-208	499	3	]	]	PUNCT
eurjchem-208	499	4	.	.	PUNCT
eurjchem-208	500	1	katcyuba	katcyuba	PROPN
eurjchem-208	500	2	,	,	PUNCT
eurjchem-208	500	3	s.	s.	PROPN
eurjchem-208	500	4	a.	a.	PROPN
eurjchem-208	500	5	;	;	PUNCT
eurjchem-208	500	6	monakhova	monakhova	PROPN
eurjchem-208	500	7	,	,	PUNCT
eurjchem-208	500	8	n.	n.	PROPN
eurjchem-208	500	9	i.	i.	PROPN
eurjchem-208	500	10	;	;	PUNCT
eurjchem-208	500	11	ashrafullina	ashrafullina	PROPN
eurjchem-208	500	12	,	,	PUNCT
eurjchem-208	500	13	l.	l.	PROPN
eurjchem-208	500	14	k.	k.	PROPN
eurjchem-208	500	15	;	;	PUNCT
eurjchem-208	500	16	shagidulin	shagidulin	PROPN
eurjchem-208	500	17	,	,	PUNCT
eurjchem-208	500	18	r.	r.	PROPN
eurjchem-208	500	19	r.	r.	PROPN
eurjchem-208	500	20	j.	j.	PROPN
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eurjchem-208	500	22	.	.	PROPN
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eurjchem-208	500	24	.	.	PUNCT
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eurjchem-208	500	26	,	,	PUNCT
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eurjchem-208	500	28	,	,	PUNCT
eurjchem-208	500	29	1‐21	1‐21	NUM
eurjchem-208	500	30	.	.	PUNCT
eurjchem-208	501	1	[	[	X
eurjchem-208	501	2	19	19	NUM
eurjchem-208	501	3	]	]	PUNCT
eurjchem-208	501	4	.	.	PUNCT
eurjchem-208	502	1	shagidulin	shagidulin	PROPN
eurjchem-208	502	2	,	,	PUNCT
eurjchem-208	502	3	r.	r.	PROPN
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eurjchem-208	502	5	;	;	PUNCT
eurjchem-208	502	6	ashrafullina	ashrafullina	PROPN
eurjchem-208	502	7	,	,	PUNCT
eurjchem-208	502	8	l.	l.	PROPN
eurjchem-208	502	9	k.	k.	PROPN
eurjchem-208	502	10	;	;	PUNCT
eurjchem-208	502	11	monakhova	monakhova	PROPN
eurjchem-208	502	12	,	,	PUNCT
eurjchem-208	502	13	n.	n.	PROPN
eurjchem-208	502	14	i.	i.	PROPN
eurjchem-208	502	15	;	;	PUNCT
eurjchem-208	502	16	katcyuba	katcyuba	PROPN
eurjchem-208	502	17	,	,	PUNCT
eurjchem-208	502	18	s.	s.	PROPN
eurjchem-208	502	19	a.	a.	PROPN
eurjchem-208	502	20	russ	russ	PROPN
eurjchem-208	502	21	.	.	PUNCT
eurjchem-208	503	1	j.	j.	PROPN
eurjchem-208	503	2	gen	gen	PROPN
eurjchem-208	503	3	.	.	PUNCT
eurjchem-208	504	1	chem.1997	chem.1997	PROPN
eurjchem-208	504	2	,	,	PUNCT
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eurjchem-208	504	4	,	,	PUNCT
eurjchem-208	504	5	567‐578	567‐578	PROPN
eurjchem-208	504	6	.	.	PUNCT
eurjchem-208	505	1	[	[	X
eurjchem-208	505	2	20	20	NUM
eurjchem-208	505	3	]	]	PUNCT
eurjchem-208	505	4	.	.	PUNCT
eurjchem-208	505	5	ali	ali	PROPN
eurjchem-208	505	6	,	,	PUNCT
eurjchem-208	505	7	t.	t.	PROPN
eurjchem-208	505	8	e.	e.	PROPN
eurjchem-208	505	9	arkivoc	arkivoc	PROPN
eurjchem-208	505	10	2008	2008	NUM
eurjchem-208	505	11	,	,	PUNCT
eurjchem-208	505	12	2	2	NUM
eurjchem-208	505	13	,	,	PUNCT
eurjchem-208	505	14	71‐79	71‐79	NUM
eurjchem-208	505	15	.	.	PUNCT
eurjchem-208	506	1	[	[	X
eurjchem-208	506	2	21	21	NUM
eurjchem-208	506	3	]	]	PUNCT
eurjchem-208	506	4	.	.	PUNCT
eurjchem-208	507	1	ali	ali	PROPN
eurjchem-208	507	2	,	,	PUNCT
eurjchem-208	507	3	t.	t.	PROPN
eurjchem-208	507	4	e.	e.	PROPN
eurjchem-208	507	5	;	;	PUNCT
eurjchem-208	507	6	halacheva	halacheva	PROPN
eurjchem-208	507	7	,	,	PUNCT
eurjchem-208	507	8	s.	s.	PROPN
eurjchem-208	507	9	s.	s.	PROPN
eurjchem-208	507	10	heteroatom	heteroatom	PROPN
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eurjchem-208	507	12	.	.	PUNCT
eurjchem-208	508	1	2009	2009	NUM
eurjchem-208	508	2	,	,	PUNCT
eurjchem-208	508	3	20	20	NUM
eurjchem-208	508	4	,	,	PUNCT
eurjchem-208	508	5	117‐122	117‐122	NUM
eurjchem-208	508	6	.	.	PUNCT
eurjchem-208	509	1	[	[	X
eurjchem-208	509	2	22	22	NUM
eurjchem-208	509	3	]	]	PUNCT
eurjchem-208	509	4	.	.	PUNCT
eurjchem-208	510	1	ali	ali	PROPN
eurjchem-208	510	2	,	,	PUNCT
eurjchem-208	510	3	t.	t.	PROPN
eurjchem-208	510	4	e.	e.	PROPN
eurjchem-208	510	5	phosphorus	phosphorus	PROPN
eurjchem-208	510	6	,	,	PUNCT
eurjchem-208	510	7	sulfur	sulfur	NOUN
eurjchem-208	510	8	silicon	silicon	NOUN
eurjchem-208	510	9	and	and	CCONJ
eurjchem-208	510	10	relat	relat	PROPN
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eurjchem-208	511	2	.	.	PUNCT
eurjchem-208	512	1	2010	2010	NUM
eurjchem-208	512	2	,	,	PUNCT
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eurjchem-208	512	4	,	,	PUNCT
eurjchem-208	512	5	88‐96	88‐96	ADV
eurjchem-208	512	6	.	.	PUNCT
eurjchem-208	513	1	[	[	X
eurjchem-208	513	2	23	23	NUM
eurjchem-208	513	3	]	]	PUNCT
eurjchem-208	513	4	.	.	PUNCT
eurjchem-208	513	5	shukla	shukla	PROPN
eurjchem-208	513	6	,	,	PUNCT
eurjchem-208	513	7	j.	j.	PROPN
eurjchem-208	513	8	s.	s.	PROPN
eurjchem-208	513	9	;	;	PUNCT
eurjchem-208	513	10	zaidi	zaidi	PROPN
eurjchem-208	513	11	,	,	PUNCT
eurjchem-208	513	12	mohd	mohd	PROPN
eurjchem-208	513	13	.	.	PUNCT
eurjchem-208	514	1	g.	g.	PROPN
eurjchem-208	514	2	h.	h.	PROPN
eurjchem-208	514	3	asian	asian	PROPN
eurjchem-208	514	4	j.	j.	PROPN
eurjchem-208	514	5	chem	chem	PROPN
eurjchem-208	514	6	.	.	PUNCT
eurjchem-208	515	1	1993	1993	NUM
eurjchem-208	515	2	,	,	PUNCT
eurjchem-208	515	3	5	5	NUM
eurjchem-208	515	4	,	,	PUNCT
eurjchem-208	515	5	253‐258	253‐258	NUM
eurjchem-208	515	6	.	.	PUNCT
eurjchem-208	516	1	[	[	X
eurjchem-208	516	2	24	24	NUM
eurjchem-208	516	3	]	]	PUNCT
eurjchem-208	516	4	.	.	PUNCT
eurjchem-208	517	1	corbridge	corbridge	PROPN
eurjchem-208	517	2	,	,	PUNCT
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eurjchem-208	517	5	c.	c.	PROPN
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eurjchem-208	517	13	,	,	PUNCT
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eurjchem-208	517	17	,	,	PUNCT
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eurjchem-208	517	19	edn	edn	NOUN
eurjchem-208	517	20	.	.	PUNCT
eurjchem-208	517	21	,	,	PUNCT
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eurjchem-208	517	23	,	,	PUNCT
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eurjchem-208	517	25	,	,	PUNCT
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eurjchem-208	517	27	,	,	PUNCT
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eurjchem-208	517	30	.	.	PUNCT
eurjchem-208	518	1	[	[	X
eurjchem-208	518	2	25	25	NUM
eurjchem-208	518	3	]	]	PUNCT
eurjchem-208	518	4	.	.	PUNCT
eurjchem-208	519	1	babin	babin	PROPN
eurjchem-208	519	2	,	,	PUNCT
eurjchem-208	519	3	y.	y.	PROPN
eurjchem-208	519	4	v.	v.	PROPN
eurjchem-208	519	5	;	;	PUNCT
eurjchem-208	519	6	gavrikov	gavrikov	PROPN
eurjchem-208	519	7	,	,	PUNCT
eurjchem-208	519	8	a.	a.	NOUN
eurjchem-208	519	9	v.	v.	PROPN
eurjchem-208	519	10	;	;	PUNCT
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eurjchem-208	519	12	,	,	PUNCT
eurjchem-208	519	13	y.	y.	PROPN
eurjchem-208	519	14	a.	a.	PROPN
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eurjchem-208	519	17	.	.	PUNCT
eurjchem-208	519	18	2008	2008	NUM
eurjchem-208	519	19	,	,	PUNCT
eurjchem-208	519	20	18	18	NUM
eurjchem-208	519	21	,	,	PUNCT
eurjchem-208	519	22	12‐13	12‐13	NUM
eurjchem-208	519	23	.	.	PUNCT
eurjchem-208	520	1	[	[	X
eurjchem-208	520	2	26	26	NUM
eurjchem-208	520	3	]	]	PUNCT
eurjchem-208	520	4	.	.	PUNCT
eurjchem-208	521	1	mamaev	mamaev	PROPN
eurjchem-208	521	2	,	,	PUNCT
eurjchem-208	521	3	v.	v.	ADP
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eurjchem-208	521	5	;	;	PUNCT
eurjchem-208	521	6	prisyajnuk	prisyajnuk	NOUN
eurjchem-208	521	7	,	,	PUNCT
eurjchem-208	521	8	a.	a.	NOUN
eurjchem-208	521	9	v.	v.	PROPN
eurjchem-208	521	10	;	;	PUNCT
eurjchem-208	521	11	laikov	laikov	PROPN
eurjchem-208	521	12	,	,	PUNCT
eurjchem-208	521	13	d.	d.	PROPN
eurjchem-208	521	14	n.	n.	PROPN
eurjchem-208	521	15	;	;	PUNCT
eurjchem-208	521	16	logutenko	logutenko	PROPN
eurjchem-208	521	17	,	,	PUNCT
eurjchem-208	521	18	l.	l.	PROPN
eurjchem-208	521	19	s.	s.	PROPN
eurjchem-208	521	20	;	;	PUNCT
eurjchem-208	521	21	babin	babin	PROPN
eurjchem-208	521	22	,	,	PUNCT
eurjchem-208	521	23	y.	y.	PROPN
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eurjchem-208	521	25	russ	russ	PROPN
eurjchem-208	521	26	.	.	PUNCT
eurjchem-208	522	1	j.	j.	PROPN
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eurjchem-208	522	3	.	.	PUNCT
eurjchem-208	523	1	chem	chem	PROPN
eurjchem-208	523	2	.	.	PUNCT
eurjchem-208	524	1	2001	2001	NUM
eurjchem-208	524	2	,	,	PUNCT
eurjchem-208	524	3	75	75	NUM
eurjchem-208	524	4	,	,	PUNCT
eurjchem-208	524	5	581‐588	581‐588	NUM
eurjchem-208	524	6	.	.	PUNCT
eurjchem-208	525	1	[	[	X
eurjchem-208	525	2	27	27	NUM
eurjchem-208	525	3	]	]	PUNCT
eurjchem-208	525	4	.	.	PUNCT
eurjchem-208	526	1	mamaev	mamaev	PROPN
eurjchem-208	526	2	,	,	PUNCT
eurjchem-208	526	3	v.	v.	ADP
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eurjchem-208	526	5	;	;	PUNCT
eurjchem-208	526	6	prisyajnuk	prisyajnuk	NOUN
eurjchem-208	526	7	,	,	PUNCT
eurjchem-208	526	8	a.	a.	NOUN
eurjchem-208	526	9	v.	v.	PROPN
eurjchem-208	526	10	;	;	PUNCT
eurjchem-208	526	11	logutenko	logutenko	PROPN
eurjchem-208	526	12	,	,	PUNCT
eurjchem-208	526	13	l.	l.	PROPN
eurjchem-208	526	14	s.	s.	PROPN
eurjchem-208	526	15	;	;	PUNCT
eurjchem-208	526	16	babin	babin	PROPN
eurjchem-208	526	17	,	,	PUNCT
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eurjchem-208	526	20	mendeleev	mendeleev	PROPN
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eurjchem-208	526	22	.	.	PUNCT
eurjchem-208	527	1	2001	2001	NUM
eurjchem-208	527	2	,	,	PUNCT
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eurjchem-208	527	4	,	,	PUNCT
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eurjchem-208	527	6	.	.	PUNCT
eurjchem-208	528	1	[	[	X
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eurjchem-208	528	3	]	]	PUNCT
eurjchem-208	528	4	.	.	PUNCT
eurjchem-208	529	1	maffei	maffei	PROPN
eurjchem-208	529	2	,	,	PUNCT
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eurjchem-208	529	4	;	;	PUNCT
eurjchem-208	529	5	buono	buono	PROPN
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eurjchem-208	530	1	[	[	X
eurjchem-208	530	2	29	29	NUM
eurjchem-208	530	3	]	]	PUNCT
eurjchem-208	530	4	.	.	PUNCT
eurjchem-208	530	5	brehme	brehme	PROPN
eurjchem-208	530	6	,	,	PUNCT
eurjchem-208	530	7	r.	r.	PROPN
eurjchem-208	530	8	;	;	PUNCT
eurjchem-208	530	9	grundemann	grundemann	PROPN
eurjchem-208	530	10	,	,	PUNCT
eurjchem-208	530	11	e.	e.	PROPN
eurjchem-208	530	12	;	;	PUNCT
eurjchem-208	530	13	schneider	schneider	PROPN
eurjchem-208	530	14	,	,	PUNCT
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eurjchem-208	530	16	j.	j.	PROPN
eurjchem-208	530	17	prakt	prakt	PROPN
eurjchem-208	530	18	.	.	PUNCT
eurjchem-208	531	1	chem	chem	NOUN
eurjchem-208	531	2	.	.	PUNCT
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eurjchem-208	532	2	,	,	PUNCT
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eurjchem-208	532	4	,	,	PUNCT
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eurjchem-208	532	6	.	.	PUNCT
eurjchem-208	533	1	[	[	X
eurjchem-208	533	2	30	30	NUM
eurjchem-208	533	3	]	]	PUNCT
eurjchem-208	533	4	.	.	PUNCT
eurjchem-208	534	1	rathelot	rathelot	NOUN
eurjchem-208	534	2	,	,	PUNCT
eurjchem-208	534	3	p.	p.	NOUN
eurjchem-208	534	4	;	;	PUNCT
eurjchem-208	534	5	azas	aza	NOUN
eurjchem-208	534	6	,	,	PUNCT
eurjchem-208	534	7	n.	n.	NOUN
eurjchem-208	534	8	;	;	PUNCT
eurjchem-208	534	9	el‐kashef	el‐kashef	PROPN
eurjchem-208	534	10	,	,	PUNCT
eurjchem-208	534	11	h.	h.	PROPN
eurjchem-208	534	12	;	;	PUNCT
eurjchem-208	534	13	delmas	delmas	PROPN
eurjchem-208	534	14	,	,	PUNCT
eurjchem-208	534	15	f.	f.	PROPN
eurjchem-208	534	16	;	;	PUNCT
eurjchem-208	534	17	di	di	X
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eurjchem-208	534	19	,	,	PUNCT
eurjchem-208	534	20	c.	c.	PROPN
eurjchem-208	534	21	;	;	PUNCT
eurjchem-208	534	22	timon‐	timon‐	PROPN
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eurjchem-208	534	24	,	,	PUNCT
eurjchem-208	534	25	p.	p.	PROPN
eurjchem-208	534	26	;	;	PUNCT
eurjchem-208	534	27	maldonado	maldonado	PROPN
eurjchem-208	534	28	,	,	PUNCT
eurjchem-208	534	29	j.	j.	PROPN
eurjchem-208	534	30	;	;	PUNCT
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eurjchem-208	535	1	j.	j.	PROPN
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eurjchem-208	535	3	.	.	PROPN
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eurjchem-208	535	5	.	.	PUNCT
eurjchem-208	536	1	2002	2002	NUM
eurjchem-208	536	2	,	,	PUNCT
eurjchem-208	536	3	37	37	NUM
eurjchem-208	536	4	,	,	PUNCT
eurjchem-208	536	5	671‐	671‐	NUM
eurjchem-208	536	6	679	679	NUM
eurjchem-208	536	7	.	.	PUNCT
eurjchem-208	537	1	[	[	X
eurjchem-208	537	2	31	31	NUM
eurjchem-208	537	3	]	]	PUNCT
eurjchem-208	537	4	.	.	PUNCT
eurjchem-208	538	1	abadi	abadi	PROPN
eurjchem-208	538	2	,	,	PUNCT
eurjchem-208	538	3	a.	a.	PROPN
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eurjchem-208	538	5	;	;	PUNCT
eurjchem-208	538	6	eissa	eissa	ADJ
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eurjchem-208	538	13	,	,	PUNCT
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eurjchem-208	538	15	s.	s.	PROPN
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eurjchem-208	538	17	.	.	PUNCT
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eurjchem-208	539	2	.	.	PUNCT
eurjchem-208	540	1	bull	bull	PROPN
eurjchem-208	540	2	.	.	PUNCT
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eurjchem-208	541	2	,	,	PUNCT
eurjchem-208	541	3	51	51	NUM
eurjchem-208	541	4	,	,	PUNCT
eurjchem-208	541	5	838‐844	838‐844	NUM
eurjchem-208	541	6	.	.	PUNCT
eurjchem-208	542	1	[	[	X
eurjchem-208	542	2	32	32	NUM
eurjchem-208	542	3	]	]	PUNCT
eurjchem-208	542	4	.	.	PUNCT
eurjchem-208	543	1	de	de	X
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eurjchem-208	543	3	,	,	PUNCT
eurjchem-208	543	4	l.	l.	PROPN
eurjchem-208	543	5	;	;	PUNCT
eurjchem-208	543	6	giaocomelli	giaocomelli	PROPN
eurjchem-208	543	7	,	,	PUNCT
eurjchem-208	543	8	g.	g.	PROPN
eurjchem-208	543	9	;	;	PUNCT
eurjchem-208	543	10	masala	masala	PROPN
eurjchem-208	543	11	,	,	PUNCT
eurjchem-208	543	12	s.	s.	PROPN
eurjchem-208	543	13	;	;	PUNCT
eurjchem-208	543	14	porcheddu	porcheddu	VERB
eurjchem-208	543	15	,	,	PUNCT
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eurjchem-208	543	17	a.	a.	NOUN
eurjchem-208	543	18	synlett.2004	synlett.2004	PROPN
eurjchem-208	543	19	,	,	PUNCT
eurjchem-208	543	20	13	13	NUM
eurjchem-208	543	21	,	,	PUNCT
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eurjchem-208	543	23	.	.	PUNCT
eurjchem-208	544	1	[	[	X
eurjchem-208	544	2	33	33	NUM
eurjchem-208	544	3	]	]	PUNCT
eurjchem-208	544	4	.	.	PUNCT
eurjchem-208	545	1	kumar	kumar	PROPN
eurjchem-208	545	2	,	,	PUNCT
eurjchem-208	545	3	a.	a.	PROPN
eurjchem-208	545	4	;	;	PUNCT
eurjchem-208	545	5	prakash	prakash	PROPN
eurjchem-208	545	6	,	,	PUNCT
eurjchem-208	545	7	o.	o.	PROPN
eurjchem-208	545	8	;	;	PUNCT
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eurjchem-208	545	10	,	,	PUNCT
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eurjchem-208	545	12	;	;	PUNCT
eurjchem-208	545	13	singh	singh	PROPN
eurjchem-208	545	14	,	,	PUNCT
eurjchem-208	545	15	s.	s.	PROPN
eurjchem-208	545	16	p.	p.	PROPN
eurjchem-208	545	17	can	can	AUX
eurjchem-208	545	18	.	.	PUNCT
eurjchem-208	546	1	j.	j.	PROPN
eurjchem-208	546	2	chem	chem	PROPN
eurjchem-208	546	3	.	.	PUNCT
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eurjchem-208	547	2	,	,	PUNCT
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eurjchem-208	547	4	,	,	PUNCT
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eurjchem-208	547	6	.	.	PUNCT
eurjchem-208	548	1	abdel‐aziz	abdel‐aziz	INTJ
eurjchem-208	549	1	et	et	PROPN
eurjchem-208	549	2	al./	al./	ADV
eurjchem-208	549	3	european	european	PROPN
eurjchem-208	549	4	journal	journal	PROPN
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eurjchem-208	549	7	2	2	NUM
eurjchem-208	549	8	(	(	PUNCT
eurjchem-208	549	9	1	1	NUM
eurjchem-208	549	10	)	)	PUNCT
eurjchem-208	549	11	(	(	PUNCT
eurjchem-208	549	12	2011	2011	NUM
eurjchem-208	549	13	)	)	PUNCT
eurjchem-208	549	14	25‐35	25‐35	NUM
eurjchem-208	549	15	35	35	NUM
eurjchem-208	550	1	[	[	X
eurjchem-208	550	2	34	34	NUM
eurjchem-208	550	3	]	]	PUNCT
eurjchem-208	550	4	.	.	PUNCT
eurjchem-208	551	1	sosnovskikh	sosnovskikh	PROPN
eurjchem-208	551	2	,	,	PUNCT
eurjchem-208	551	3	v.	v.	PROPN
eurjchem-208	551	4	y.	y.	PROPN
eurjchem-208	551	5	;	;	PUNCT
eurjchem-208	551	6	kutsenko	kutsenko	PROPN
eurjchem-208	551	7	,	,	PUNCT
eurjchem-208	551	8	v.	v.	PROPN
eurjchem-208	551	9	a.	a.	NOUN
eurjchem-208	551	10	;	;	PUNCT
eurjchem-208	551	11	ovsyannikov	ovsyannikov	PROPN
eurjchem-208	551	12	,	,	PUNCT
eurjchem-208	551	13	i.	i.	PROPN
eurjchem-208	551	14	s.	s.	PROPN
eurjchem-208	551	15	russ	russ	PROPN
eurjchem-208	551	16	.	.	PROPN
eurjchem-208	552	1	chem	chem	PROPN
eurjchem-208	552	2	.	.	PUNCT
eurjchem-208	553	1	bull	bull	NOUN
eurjchem-208	553	2	.	.	PUNCT
eurjchem-208	554	1	2000	2000	NUM
eurjchem-208	554	2	,	,	PUNCT
eurjchem-208	554	3	49	49	NUM
eurjchem-208	554	4	,	,	PUNCT
eurjchem-208	554	5	478‐481	478‐481	NUM
eurjchem-208	554	6	.	.	PUNCT
eurjchem-208	555	1	[	[	X
eurjchem-208	555	2	35	35	NUM
eurjchem-208	555	3	]	]	PUNCT
eurjchem-208	555	4	.	.	PUNCT
eurjchem-208	556	1	abdel‐khalik	abdel‐khalik	PROPN
eurjchem-208	556	2	,	,	PUNCT
eurjchem-208	556	3	m.	m.	NOUN
eurjchem-208	556	4	m.	m.	NOUN
eurjchem-208	556	5	;	;	PUNCT
eurjchem-208	556	6	negm	negm	PROPN
eurjchem-208	556	7	,	,	PUNCT
eurjchem-208	556	8	a.	a.	NOUN
eurjchem-208	556	9	m.	m.	NOUN
eurjchem-208	556	10	;	;	PUNCT
eurjchem-208	556	11	elkhouly	elkhouly	ADV
eurjchem-208	556	12	,	,	PUNCT
eurjchem-208	556	13	a.	a.	NOUN
eurjchem-208	556	14	i.	i.	PROPN
eurjchem-208	556	15	,	,	PUNCT
eurjchem-208	556	16	elnagdi	elnagdi	PROPN
eurjchem-208	556	17	,	,	PUNCT
eurjchem-208	556	18	m.	m.	NOUN
eurjchem-208	556	19	h.	h.	PROPN
eurjchem-208	556	20	heteroatom	heteroatom	PROPN
eurjchem-208	556	21	chem	chem	PROPN
eurjchem-208	556	22	.	.	PUNCT
eurjchem-208	557	1	2004	2004	NUM
eurjchem-208	557	2	,	,	PUNCT
eurjchem-208	557	3	15	15	NUM
eurjchem-208	557	4	,	,	PUNCT
eurjchem-208	557	5	502‐507	502‐507	NUM
eurjchem-208	557	6	.	.	PUNCT
eurjchem-208	558	1	[	[	X
eurjchem-208	558	2	36	36	NUM
eurjchem-208	558	3	]	]	PUNCT
eurjchem-208	558	4	.	.	PUNCT
eurjchem-208	559	1	ghosh	ghosh	PROPN
eurjchem-208	559	2	,	,	PUNCT
eurjchem-208	559	3	c.	c.	PROPN
eurjchem-208	559	4	k.	k.	PROPN
eurjchem-208	559	5	;	;	PUNCT
eurjchem-208	559	6	sahana	sahana	PROPN
eurjchem-208	559	7	,	,	PUNCT
eurjchem-208	559	8	s.	s.	PROPN
eurjchem-208	559	9	tetrahedron	tetrahedron	PROPN
eurjchem-208	559	10	1993	1993	NUM
eurjchem-208	559	11	,	,	PUNCT
eurjchem-208	559	12	49	49	NUM
eurjchem-208	559	13	,	,	PUNCT
eurjchem-208	559	14	4127‐4134	4127‐4134	NUM
eurjchem-208	559	15	.	.	PUNCT
eurjchem-208	560	1	[	[	X
eurjchem-208	560	2	37	37	NUM
eurjchem-208	560	3	]	]	PUNCT
eurjchem-208	560	4	.	.	PUNCT
eurjchem-208	561	1	rakitin	rakitin	NOUN
eurjchem-208	561	2	,	,	PUNCT
eurjchem-208	561	3	o.	o.	PROPN
eurjchem-208	561	4	a.	a.	NOUN
eurjchem-208	561	5	arkivoc	arkivoc	PROPN
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eurjchem-208	561	7	,	,	PUNCT
eurjchem-208	561	8	1	1	NUM
eurjchem-208	561	9	,	,	PUNCT
eurjchem-208	561	10	129‐149	129‐149	NUM
eurjchem-208	561	11	.	.	PUNCT
eurjchem-208	562	1	[	[	X
eurjchem-208	562	2	38	38	NUM
eurjchem-208	562	3	]	]	PUNCT
eurjchem-208	562	4	.	.	PUNCT
eurjchem-208	563	1	hudson	hudson	PROPN
eurjchem-208	563	2	,	,	PUNCT
eurjchem-208	563	3	h.	h.	PROPN
eurjchem-208	563	4	r.	r.	PROPN
eurjchem-208	563	5	;	;	PUNCT
eurjchem-208	563	6	keglevich	keglevich	PROPN
eurjchem-208	563	7	,	,	PUNCT
eurjchem-208	563	8	g.	g.	PROPN
eurjchem-208	563	9	phosphorus	phosphorus	NOUN
eurjchem-208	563	10	,	,	PUNCT
eurjchem-208	563	11	sulfur	sulfur	NOUN
eurjchem-208	563	12	silicon	silicon	NOUN
eurjchem-208	563	13	and	and	CCONJ
eurjchem-208	563	14	relat	relat	PROPN
eurjchem-208	563	15	.	.	PUNCT
eurjchem-208	564	1	elem	elem	NOUN
eurjchem-208	564	2	.	.	PUNCT
eurjchem-208	565	1	2008	2008	NUM
eurjchem-208	565	2	,	,	PUNCT
eurjchem-208	565	3	183	183	NUM
eurjchem-208	565	4	,	,	PUNCT
eurjchem-208	565	5	2256‐2261	2256‐2261	NOUN
eurjchem-208	565	6	.	.	PUNCT
eurjchem-208	566	1	[	[	X
eurjchem-208	566	2	39	39	NUM
eurjchem-208	566	3	]	]	PUNCT
eurjchem-208	566	4	.	.	PUNCT
eurjchem-208	567	1	babu	babu	PROPN
eurjchem-208	567	2	,	,	PUNCT
eurjchem-208	567	3	b.	b.	PROPN
eurjchem-208	567	4	h.	h.	PROPN
eurjchem-208	567	5	;	;	PUNCT
eurjchem-208	567	6	sirinivasulu	sirinivasulu	VERB
eurjchem-208	567	7	,	,	PUNCT
eurjchem-208	567	8	k.	k.	PROPN
eurjchem-208	567	9	;	;	PUNCT
eurjchem-208	568	1	babu	babu	PROPN
eurjchem-208	568	2	,	,	PUNCT
eurjchem-208	568	3	b.	b.	PROPN
eurjchem-208	568	4	v.	v.	PROPN
eurjchem-208	568	5	;	;	PUNCT
eurjchem-208	568	6	sirinivas	sirinivas	PROPN
eurjchem-208	568	7	,	,	PUNCT
eurjchem-208	568	8	r.	r.	PROPN
eurjchem-208	568	9	;	;	PUNCT
eurjchem-208	568	10	raju	raju	PROPN
eurjchem-208	568	11	,	,	PUNCT
eurjchem-208	568	12	c.	c.	PROPN
eurjchem-208	568	13	n.	n.	PROPN
eurjchem-208	568	14	synth	synth	PROPN
eurjchem-208	568	15	.	.	PUNCT
eurjchem-208	569	1	commun.2008	commun.2008	NOUN
eurjchem-208	569	2	,	,	PUNCT
eurjchem-208	569	3	38	38	NUM
eurjchem-208	569	4	,	,	PUNCT
eurjchem-208	569	5	2941‐2949	2941‐2949	NUM
eurjchem-208	569	6	.	.	PUNCT
eurjchem-208	570	1	[	[	X
eurjchem-208	570	2	40	40	NUM
eurjchem-208	570	3	]	]	PUNCT
eurjchem-208	570	4	.	.	PUNCT
eurjchem-208	571	1	petteren	petteren	PROPN
eurjchem-208	571	2	,	,	PUNCT
eurjchem-208	571	3	d.	d.	PROPN
eurjchem-208	571	4	;	;	PUNCT
eurjchem-208	571	5	marcolini	marcolini	NOUN
eurjchem-208	571	6	,	,	PUNCT
eurjchem-208	571	7	m.	m.	NOUN
eurjchem-208	571	8	;	;	PUNCT
eurjchem-208	571	9	bernardi	bernardi	PROPN
eurjchem-208	571	10	,	,	PUNCT
eurjchem-208	571	11	l.	l.	PROPN
eurjchem-208	571	12	;	;	PUNCT
eurjchem-208	571	13	fini	fini	PROPN
eurjchem-208	571	14	,	,	PUNCT
eurjchem-208	571	15	f.	f.	PROPN
eurjchem-208	571	16	;	;	PUNCT
eurjchem-208	571	17	herrera	herrera	PROPN
eurjchem-208	571	18	,	,	PUNCT
eurjchem-208	571	19	r.	r.	PROPN
eurjchem-208	571	20	;	;	PUNCT
eurjchem-208	571	21	sgarzani	sgarzani	PROPN
eurjchem-208	571	22	,	,	PUNCT
eurjchem-208	571	23	v.	v.	ADP
eurjchem-208	571	24	;	;	PUNCT
eurjchem-208	571	25	ricci	ricci	PROPN
eurjchem-208	571	26	,	,	PUNCT
eurjchem-208	571	27	a.	a.	PROPN
eurjchem-208	571	28	j.	j.	PROPN
eurjchem-208	571	29	org	org	PROPN
eurjchem-208	571	30	.	.	PUNCT
eurjchem-208	571	31	chem	chem	PROPN
eurjchem-208	571	32	.	.	PUNCT
eurjchem-208	572	1	2006	2006	NUM
eurjchem-208	572	2	,	,	PUNCT
eurjchem-208	572	3	71	71	NUM
eurjchem-208	572	4	,	,	PUNCT
eurjchem-208	572	5	6269‐6272	6269‐6272	NOUN
eurjchem-208	572	6	.	.	PUNCT
eurjchem-208	573	1	[	[	X
eurjchem-208	573	2	41	41	NUM
eurjchem-208	573	3	]	]	PUNCT
eurjchem-208	573	4	.	.	PUNCT
eurjchem-208	574	1	failla	failla	PROPN
eurjchem-208	574	2	,	,	PUNCT
eurjchem-208	574	3	s.	s.	PROPN
eurjchem-208	574	4	;	;	PUNCT
eurjchem-208	574	5	finocchiaro	finocchiaro	PROPN
eurjchem-208	574	6	,	,	PUNCT
eurjchem-208	574	7	p.	p.	NOUN
eurjchem-208	574	8	;	;	PUNCT
eurjchem-208	574	9	hagele	hagele	PROPN
eurjchem-208	574	10	,	,	PUNCT
eurjchem-208	574	11	g.	g.	PROPN
eurjchem-208	574	12	;	;	PUNCT
eurjchem-208	574	13	rapisardi	rapisardi	PROPN
eurjchem-208	574	14	,	,	PUNCT
eurjchem-208	574	15	r.	r.	NOUN
eurjchem-208	574	16	phosphorus	phosphorus	NOUN
eurjchem-208	574	17	,	,	PUNCT
eurjchem-208	574	18	sulfur	sulfur	NOUN
eurjchem-208	574	19	silicon	silicon	NOUN
eurjchem-208	574	20	and	and	CCONJ
eurjchem-208	574	21	relat	relat	PROPN
eurjchem-208	574	22	.	.	PUNCT
eurjchem-208	575	1	elem	elem	NOUN
eurjchem-208	575	2	.	.	PUNCT
eurjchem-208	576	1	1993	1993	NUM
eurjchem-208	576	2	,	,	PUNCT
eurjchem-208	576	3	82	82	NUM
eurjchem-208	576	4	,	,	PUNCT
eurjchem-208	576	5	79‐89	79‐89	NUM
eurjchem-208	576	6	.	.	PUNCT
eurjchem-208	577	1	[	[	X
eurjchem-208	577	2	42	42	NUM
eurjchem-208	577	3	]	]	PUNCT
eurjchem-208	577	4	.	.	PUNCT
eurjchem-208	578	1	kumar	kumar	PROPN
eurjchem-208	578	2	,	,	PUNCT
eurjchem-208	578	3	s.	s.	PROPN
eurjchem-208	578	4	k.	k.	PROPN
eurjchem-208	578	5	;	;	PUNCT
eurjchem-208	578	6	hager	hager	PROPN
eurjchem-208	578	7	,	,	PUNCT
eurjchem-208	578	8	e.	e.	PROPN
eurjchem-208	578	9	;	;	PUNCT
eurjchem-208	578	10	pettit	pettit	PROPN
eurjchem-208	578	11	,	,	PUNCT
eurjchem-208	578	12	c.	c.	PROPN
eurjchem-208	578	13	;	;	PUNCT
eurjchem-208	578	14	gurulingappa	gurulingappa	PROPN
eurjchem-208	578	15	,	,	PUNCT
eurjchem-208	578	16	h.	h.	PROPN
eurjchem-208	578	17	;	;	PUNCT
eurjchem-208	578	18	davidson	davidson	PROPN
eurjchem-208	578	19	,	,	PUNCT
eurjchem-208	578	20	n.	n.	PROPN
eurjchem-208	578	21	e.	e.	PROPN
eurjchem-208	578	22	;	;	PUNCT
eurjchem-208	578	23	khan	khan	PROPN
eurjchem-208	578	24	,	,	PUNCT
eurjchem-208	578	25	s.	s.	PROPN
eurjchem-208	578	26	r.	r.	PROPN
eurjchem-208	578	27	j.	j.	PROPN
eurjchem-208	578	28	med	med	PROPN
eurjchem-208	578	29	.	.	PROPN
eurjchem-208	578	30	chem	chem	PROPN
eurjchem-208	578	31	.	.	PUNCT
eurjchem-208	579	1	2003	2003	NUM
eurjchem-208	579	2	,	,	PUNCT
eurjchem-208	579	3	46	46	NUM
eurjchem-208	579	4	,	,	PUNCT
eurjchem-208	579	5	2813‐2815	2813‐2815	NUM
eurjchem-208	579	6	.	.	PUNCT
eurjchem-208	580	1	[	[	X
eurjchem-208	580	2	43	43	NUM
eurjchem-208	580	3	]	]	PUNCT
eurjchem-208	580	4	.	.	PUNCT
eurjchem-208	581	1	wu	wu	PROPN
eurjchem-208	581	2	,	,	PUNCT
eurjchem-208	581	3	j.	j.	PROPN
eurjchem-208	581	4	h.	h.	PROPN
eurjchem-208	581	5	;	;	PUNCT
eurjchem-208	581	6	wang	wang	PROPN
eurjchem-208	581	7	,	,	PUNCT
eurjchem-208	581	8	x.	x.	PROPN
eurjchem-208	581	9	h.	h.	PROPN
eurjchem-208	581	10	;	;	PUNCT
eurjchem-208	581	11	yi	yi	PROPN
eurjchem-208	581	12	,	,	PUNCT
eurjchem-208	581	13	y.	y.	PROPN
eurjchem-208	581	14	h.	h.	PROPN
eurjchem-208	581	15	;	;	PUNCT
eurjchem-208	581	16	lee	lee	PROPN
eurjchem-208	581	17	,	,	PUNCT
eurjchem-208	581	18	k.	k.	PROPN
eurjchem-208	581	19	h.	h.	PROPN
eurjchem-208	581	20	bioorg	bioorg	PROPN
eurjchem-208	581	21	.	.	PUNCT
eurjchem-208	582	1	med	med	PROPN
eurjchem-208	582	2	.	.	PROPN
eurjchem-208	582	3	chem	chem	PROPN
eurjchem-208	582	4	.	.	PUNCT
eurjchem-208	583	1	lett	lett	PROPN
eurjchem-208	583	2	.	.	PROPN
eurjchem-208	583	3	2003	2003	NUM
eurjchem-208	583	4	,	,	PUNCT
eurjchem-208	583	5	13	13	NUM
eurjchem-208	583	6	,	,	PUNCT
eurjchem-208	583	7	1813‐1815	1813‐1815	NUM
eurjchem-208	583	8	.	.	PUNCT
eurjchem-208	584	1	[	[	X
eurjchem-208	584	2	44	44	NUM
eurjchem-208	584	3	]	]	PUNCT
eurjchem-208	584	4	.	.	PUNCT
eurjchem-208	585	1	taber	taber	PROPN
eurjchem-208	585	2	,	,	PUNCT
eurjchem-208	585	3	d.	d.	PROPN
eurjchem-208	585	4	f.	f.	PROPN
eurjchem-208	585	5	;	;	PUNCT
eurjchem-208	585	6	nelson	nelson	PROPN
eurjchem-208	585	7	,	,	PUNCT
eurjchem-208	585	8	c.	c.	PROPN
eurjchem-208	585	9	g.	g.	PROPN
eurjchem-208	585	10	j.	j.	PROPN
eurjchem-208	585	11	org	org	PROPN
eurjchem-208	585	12	.	.	PUNCT
eurjchem-208	585	13	chem	chem	PROPN
eurjchem-208	585	14	.	.	PUNCT
eurjchem-208	586	1	2006	2006	NUM
eurjchem-208	586	2	,	,	PUNCT
eurjchem-208	586	3	71	71	NUM
eurjchem-208	586	4	,	,	PUNCT
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eurjchem-208	586	6	.	.	PUNCT
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eurjchem-208	589	1	[	[	X
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eurjchem-208	591	3	]	]	PUNCT
eurjchem-208	591	4	.	.	PUNCT
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eurjchem-208	599	3	,	,	PUNCT
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eurjchem-208	599	7	.	.	PUNCT
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eurjchem-208	600	3	]	]	PUNCT
eurjchem-208	600	4	.	.	PUNCT
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eurjchem-208	602	4	.	.	PUNCT
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