id sid tid token lemma pos eurjchem-224 1 1 microsoft microsoft PROPN eurjchem-224 1 2 word word NOUN eurjchem-224 1 3 european_journal_of_chemistry_1_4_2010_319_321_224 european_journal_of_chemistry_1_4_2010_319_321_224 PROPN eurjchem-224 1 4 european european ADJ eurjchem-224 1 5     SPACE eurjchem-224 1 6 journal journal NOUN eurjchem-224 1 7     SPACE eurjchem-224 1 8 of of ADP eurjchem-224 1 9     SPACE eurjchem-224 1 10 chemistry chemistry NOUN eurjchem-224 1 11     SPACE eurjchem-224 1 12 1 1 NUM eurjchem-224 1 13     SPACE eurjchem-224 1 14 ( ( PUNCT eurjchem-224 1 15 4 4 NUM eurjchem-224 1 16 ) ) PUNCT eurjchem-224 1 17     SPACE eurjchem-224 1 18 ( ( PUNCT eurjchem-224 1 19 2010 2010 NUM eurjchem-224 1 20 ) ) PUNCT eurjchem-224 1 21     SPACE eurjchem-224 1 22 319‐321 319‐321 NUM eurjchem-224 1 23         SPACE eurjchem-224 1 24 european european ADJ eurjchem-224 1 25     SPACE eurjchem-224 1 26 journal journal NOUN eurjchem-224 1 27     SPACE eurjchem-224 1 28 of of ADP eurjchem-224 1 29     SPACE eurjchem-224 1 30 chemistry chemistry NOUN eurjchem-224 1 31     SPACE eurjchem-224 1 32 issn issn VERB eurjchem-224 1 33     SPACE eurjchem-224 1 34 2153‐2249 2153‐2249 NUM eurjchem-224 1 35     SPACE eurjchem-224 1 36 ( ( PUNCT eurjchem-224 1 37 print print NOUN eurjchem-224 1 38 ) ) PUNCT eurjchem-224 1 39     SPACE eurjchem-224 1 40 / / SYM eurjchem-224 1 41     SPACE eurjchem-224 1 42 issn issn VERB eurjchem-224 1 43     SPACE eurjchem-224 1 44 2153‐2257 2153‐2257 NUM eurjchem-224 1 45     SPACE eurjchem-224 1 46 ( ( PUNCT eurjchem-224 1 47 online online ADJ eurjchem-224 1 48 ) ) PUNCT eurjchem-224 1 49     SPACE eurjchem-224 1 50   NOUN eurjchem-224 1 51     SPACE eurjchem-224 1 52 2010 2010 NUM eurjchem-224 1 53     SPACE eurjchem-224 1 54 eurjchem eurjchem NOUN eurjchem-224 1 55     SPACE eurjchem-224 1 56 doi:10.5155 doi:10.5155 PROPN eurjchem-224 1 57 / / SYM eurjchem-224 1 58 eurjchem.1.4.319‐321.224 eurjchem.1.4.319‐321.224 NOUN eurjchem-224 1 59                 SPACE eurjchem-224 1 60 european european ADJ eurjchem-224 1 61     SPACE eurjchem-224 1 62 journal journal NOUN eurjchem-224 1 63     SPACE eurjchem-224 1 64 of of ADP eurjchem-224 1 65     SPACE eurjchem-224 1 66 chemistry chemistry NOUN eurjchem-224 1 67     SPACE eurjchem-224 1 68 journal journal NOUN eurjchem-224 1 69     SPACE eurjchem-224 1 70 homepage homepage NOUN eurjchem-224 1 71 : : PUNCT eurjchem-224 1 72     SPACE eurjchem-224 1 73 www.eurjchem.com www.eurjchem.com NOUN eurjchem-224 1 74                     SPACE eurjchem-224 1 75 determination determination NOUN eurjchem-224 1 76     SPACE eurjchem-224 1 77 of of ADP eurjchem-224 1 78     SPACE eurjchem-224 1 79 enantiomeric enantiomeric ADJ eurjchem-224 1 80     SPACE eurjchem-224 1 81 excess excess NOUN eurjchem-224 1 82     SPACE eurjchem-224 1 83 of of ADP eurjchem-224 1 84     SPACE eurjchem-224 1 85 leucine leucine NOUN eurjchem-224 1 86     SPACE eurjchem-224 1 87 and and CCONJ eurjchem-224 1 88     SPACE eurjchem-224 1 89 valine valine NOUN eurjchem-224 1 90       SPACE eurjchem-224 1 91 by by ADP eurjchem-224 1 92     SPACE eurjchem-224 1 93 x‐ray x‐ray NOUN eurjchem-224 1 94     SPACE eurjchem-224 1 95 powder powder NOUN eurjchem-224 1 96     SPACE eurjchem-224 1 97 diffraction diffraction NOUN eurjchem-224 1 98     SPACE eurjchem-224 1 99 elżbieta elżbieta PROPN eurjchem-224 1 100     SPACE eurjchem-224 1 101 tadeusiaka tadeusiaka PRON eurjchem-224 1 102 , , PUNCT eurjchem-224 1 103     SPACE eurjchem-224 1 104 rafal rafal PROPN eurjchem-224 1 105     SPACE eurjchem-224 1 106 kruszynskib kruszynskib PROPN eurjchem-224 1 107 , , PUNCT eurjchem-224 1 108 * * PUNCT eurjchem-224 1 109 , , PUNCT eurjchem-224 1 110     SPACE eurjchem-224 1 111 agata agata PROPN eurjchem-224 1 112     SPACE eurjchem-224 1 113 trzesowska‐kruszynskab trzesowska‐kruszynskab PROPN eurjchem-224 1 114 , , PUNCT eurjchem-224 1 115       SPACE eurjchem-224 1 116 tomasz tomasz NOUN eurjchem-224 1 117     SPACE eurjchem-224 1 118 sieranskib sieranskib NOUN eurjchem-224 1 119     SPACE eurjchem-224 1 120 and and CCONJ eurjchem-224 1 121     SPACE eurjchem-224 1 122 bartlomiej bartlomiej ADJ eurjchem-224 1 123     SPACE eurjchem-224 1 124 lewinskib lewinskib NOUN eurjchem-224 1 125     SPACE eurjchem-224 1 126 a a DET eurjchem-224 1 127     SPACE eurjchem-224 1 128 department department NOUN eurjchem-224 1 129     SPACE eurjchem-224 1 130 of of ADP eurjchem-224 1 131     SPACE eurjchem-224 1 132 structural structural ADJ eurjchem-224 1 133     SPACE eurjchem-224 1 134 studies study NOUN eurjchem-224 1 135 , , PUNCT eurjchem-224 1 136     SPACE eurjchem-224 1 137 centre centre NOUN eurjchem-224 1 138     SPACE eurjchem-224 1 139 of of ADP eurjchem-224 1 140     SPACE eurjchem-224 1 141 molecular molecular NOUN eurjchem-224 1 142     SPACE eurjchem-224 1 143 and and CCONJ eurjchem-224 1 144     SPACE eurjchem-224 1 145 macromolecular macromolecular NOUN eurjchem-224 1 146     SPACE eurjchem-224 1 147 studies study NOUN eurjchem-224 1 148 , , PUNCT eurjchem-224 1 149     SPACE eurjchem-224 1 150 polish polish NOUN eurjchem-224 1 151     SPACE eurjchem-224 1 152 academy academy NOUN eurjchem-224 1 153     SPACE eurjchem-224 1 154 of of ADP eurjchem-224 1 155     SPACE eurjchem-224 1 156 sciences science NOUN eurjchem-224 1 157 , , PUNCT eurjchem-224 1 158     SPACE eurjchem-224 1 159 sienkiewicza sienkiewicza ADV eurjchem-224 1 160     SPACE eurjchem-224 1 161 112 112 NUM eurjchem-224 1 162 , , PUNCT eurjchem-224 1 163     SPACE eurjchem-224 1 164 łódź łódź PROPN eurjchem-224 1 165 , , PUNCT eurjchem-224 1 166     SPACE eurjchem-224 1 167 pl­90­363 pl­90­363 NOUN eurjchem-224 1 168 , , PUNCT eurjchem-224 1 169     SPACE eurjchem-224 1 170 poland poland PROPN eurjchem-224 1 171     SPACE eurjchem-224 1 172 b b PROPN eurjchem-224 1 173     SPACE eurjchem-224 1 174 department department NOUN eurjchem-224 1 175     SPACE eurjchem-224 1 176 of of ADP eurjchem-224 1 177     SPACE eurjchem-224 1 178 x­ray x­ray ADJ eurjchem-224 1 179     SPACE eurjchem-224 1 180 crystallography crystallography NOUN eurjchem-224 1 181     SPACE eurjchem-224 1 182 and and CCONJ eurjchem-224 1 183     SPACE eurjchem-224 1 184 crystal crystal NOUN eurjchem-224 1 185     SPACE eurjchem-224 1 186 chemistry chemistry NOUN eurjchem-224 1 187 , , PUNCT eurjchem-224 1 188     SPACE eurjchem-224 1 189 institute institute NOUN eurjchem-224 1 190     SPACE eurjchem-224 1 191 of of ADP eurjchem-224 1 192     SPACE eurjchem-224 1 193 general general NOUN eurjchem-224 1 194     SPACE eurjchem-224 1 195 and and CCONJ eurjchem-224 1 196     SPACE eurjchem-224 1 197 ecological ecological ADJ eurjchem-224 1 198     SPACE eurjchem-224 1 199 chemistry chemistry NOUN eurjchem-224 1 200 , , PUNCT eurjchem-224 1 201     SPACE eurjchem-224 1 202 technical technical ADJ eurjchem-224 1 203     SPACE eurjchem-224 1 204 university university NOUN eurjchem-224 1 205     SPACE eurjchem-224 1 206 of of ADP eurjchem-224 1 207     SPACE eurjchem-224 1 208 łódź łódź PROPN eurjchem-224 1 209 , , PUNCT eurjchem-224 1 210     SPACE eurjchem-224 1 211 żeromskiego żeromskiego NOUN eurjchem-224 1 212     SPACE eurjchem-224 1 213 116 116 NUM eurjchem-224 1 214 , , PUNCT eurjchem-224 1 215     SPACE eurjchem-224 1 216 łódź łódź PROPN eurjchem-224 1 217 , , PUNCT eurjchem-224 1 218     SPACE eurjchem-224 1 219 pl­90­924 pl­90­924 NOUN eurjchem-224 1 220 , , PUNCT eurjchem-224 1 221     SPACE eurjchem-224 1 222 poland poland PROPN eurjchem-224 1 223     SPACE eurjchem-224 1 224 * * PUNCT eurjchem-224 1 225 corresponding corresponding ADJ eurjchem-224 1 226     SPACE eurjchem-224 1 227 author author NOUN eurjchem-224 1 228     SPACE eurjchem-224 1 229 at at ADP eurjchem-224 1 230 : : PUNCT eurjchem-224 1 231     SPACE eurjchem-224 1 232 department department NOUN eurjchem-224 1 233     SPACE eurjchem-224 1 234 of of ADP eurjchem-224 1 235     SPACE eurjchem-224 1 236 x­ray x­ray ADJ eurjchem-224 1 237     SPACE eurjchem-224 1 238 crystallography crystallography NOUN eurjchem-224 1 239     SPACE eurjchem-224 1 240 and and CCONJ eurjchem-224 1 241     SPACE eurjchem-224 1 242 crystal crystal NOUN eurjchem-224 1 243     SPACE eurjchem-224 1 244 chemistry chemistry NOUN eurjchem-224 1 245 , , PUNCT eurjchem-224 1 246     SPACE eurjchem-224 1 247 institute institute NOUN eurjchem-224 1 248     SPACE eurjchem-224 1 249 of of ADP eurjchem-224 1 250     SPACE eurjchem-224 1 251 general general NOUN eurjchem-224 1 252     SPACE eurjchem-224 1 253 and and CCONJ eurjchem-224 1 254     SPACE eurjchem-224 1 255 ecological ecological ADJ eurjchem-224 1 256     SPACE eurjchem-224 1 257 chemistry chemistry NOUN eurjchem-224 1 258 , , PUNCT eurjchem-224 1 259     SPACE eurjchem-224 1 260 technical technical ADJ eurjchem-224 1 261     SPACE eurjchem-224 1 262 university university NOUN eurjchem-224 1 263     SPACE eurjchem-224 1 264 of of ADP eurjchem-224 1 265     SPACE eurjchem-224 1 266 łódź łódź PROPN eurjchem-224 1 267 , , PUNCT eurjchem-224 1 268     SPACE eurjchem-224 1 269 żeromskiego żeromskiego NOUN eurjchem-224 1 270     SPACE eurjchem-224 1 271 116 116 NUM eurjchem-224 1 272 , , PUNCT eurjchem-224 1 273     SPACE eurjchem-224 1 274 łódź łódź PROPN eurjchem-224 1 275 , , PUNCT eurjchem-224 1 276     SPACE eurjchem-224 1 277 pl­90­924 pl­90­924 NOUN eurjchem-224 1 278 , , PUNCT eurjchem-224 1 279     SPACE eurjchem-224 1 280 poland poland PROPN eurjchem-224 1 281 . . PUNCT eurjchem-224 1 282     SPACE eurjchem-224 2 1 tel tel PROPN eurjchem-224 2 2 . . PUNCT eurjchem-224 2 3 : : PUNCT eurjchem-224 2 4     SPACE eurjchem-224 2 5 +48.42.6313137 +48.42.6313137 NUM eurjchem-224 2 6 ; ; PUNCT eurjchem-224 2 7     SPACE eurjchem-224 2 8 fax fax NOUN eurjchem-224 2 9 : : PUNCT eurjchem-224 2 10     SPACE eurjchem-224 2 11 +48.42.6313103 +48.42.6313103 PROPN eurjchem-224 2 12 . . PUNCT eurjchem-224 2 13     SPACE eurjchem-224 2 14 e­mail e­mail NOUN eurjchem-224 2 15     SPACE eurjchem-224 2 16 address address NOUN eurjchem-224 2 17 : : PUNCT eurjchem-224 2 18     SPACE eurjchem-224 2 19 rafal.kruszynski@p.lodz.pl rafal.kruszynski@p.lodz.pl VERB eurjchem-224 2 20     SPACE eurjchem-224 2 21 ( ( PUNCT eurjchem-224 2 22 r. r. NOUN eurjchem-224 2 23     SPACE eurjchem-224 2 24 kruszynski kruszynski PROPN eurjchem-224 2 25 ) ) PUNCT eurjchem-224 2 26 . . PUNCT eurjchem-224 2 27                                     SPACE eurjchem-224 3 1 article article NOUN eurjchem-224 3 2     SPACE eurjchem-224 3 3 information information NOUN eurjchem-224 3 4         SPACE eurjchem-224 3 5 abstract abstract ADJ eurjchem-224 3 6 received receive VERB eurjchem-224 3 7 : : PUNCT eurjchem-224 3 8     SPACE eurjchem-224 3 9 26 26 NUM eurjchem-224 3 10     SPACE eurjchem-224 3 11 june june PROPN eurjchem-224 3 12     SPACE eurjchem-224 3 13 2010 2010 NUM eurjchem-224 3 14     SPACE eurjchem-224 3 15 accepted accept VERB eurjchem-224 3 16 : : PUNCT eurjchem-224 3 17     SPACE eurjchem-224 3 18 06 06 NUM eurjchem-224 3 19     SPACE eurjchem-224 3 20 august august PROPN eurjchem-224 3 21     SPACE eurjchem-224 3 22 2010 2010 NUM eurjchem-224 3 23     SPACE eurjchem-224 3 24 online online NOUN eurjchem-224 3 25 : : PUNCT eurjchem-224 3 26     SPACE eurjchem-224 3 27 31 31 NUM eurjchem-224 3 28     SPACE eurjchem-224 3 29 december december PROPN eurjchem-224 3 30     SPACE eurjchem-224 3 31 2010 2010 NUM eurjchem-224 3 32     SPACE eurjchem-224 3 33 keywords keyword VERB eurjchem-224 3 34         SPACE eurjchem-224 3 35 two two NUM eurjchem-224 3 36     SPACE eurjchem-224 3 37 amino amino NOUN eurjchem-224 3 38     SPACE eurjchem-224 3 39 acids acid NOUN eurjchem-224 3 40 , , PUNCT eurjchem-224 3 41     SPACE eurjchem-224 3 42 leucine leucine NOUN eurjchem-224 3 43     SPACE eurjchem-224 3 44 and and CCONJ eurjchem-224 3 45     SPACE eurjchem-224 3 46 valine valine NOUN eurjchem-224 3 47 , , PUNCT eurjchem-224 3 48     SPACE eurjchem-224 3 49 were be AUX eurjchem-224 3 50     SPACE eurjchem-224 3 51 studied study VERB eurjchem-224 3 52     SPACE eurjchem-224 3 53 by by ADP eurjchem-224 3 54     SPACE eurjchem-224 3 55 x‐ray x‐ray NOUN eurjchem-224 3 56     SPACE eurjchem-224 3 57 powder powder NOUN eurjchem-224 3 58     SPACE eurjchem-224 3 59 diffraction diffraction NOUN eurjchem-224 3 60     SPACE eurjchem-224 3 61 ( ( PUNCT eurjchem-224 3 62 xrpd xrpd PROPN eurjchem-224 3 63 ) ) PUNCT eurjchem-224 3 64 . . PUNCT eurjchem-224 3 65     SPACE eurjchem-224 4 1 the the DET eurjchem-224 4 2     SPACE eurjchem-224 4 3 linear linear ADJ eurjchem-224 4 4     SPACE eurjchem-224 4 5 correlations correlation NOUN eurjchem-224 4 6     SPACE eurjchem-224 4 7 between between ADP eurjchem-224 4 8     SPACE eurjchem-224 4 9 intensity intensity NOUN eurjchem-224 4 10     SPACE eurjchem-224 4 11 of of ADP eurjchem-224 4 12     SPACE eurjchem-224 4 13 racemate racemate VERB eurjchem-224 4 14     SPACE eurjchem-224 4 15 ( ( PUNCT eurjchem-224 4 16 decrease decrease NOUN eurjchem-224 4 17 ) ) PUNCT eurjchem-224 4 18     SPACE eurjchem-224 4 19 or or CCONJ eurjchem-224 4 20     SPACE eurjchem-224 4 21 enantiomer enantiomer NOUN eurjchem-224 4 22     SPACE eurjchem-224 4 23 ( ( PUNCT eurjchem-224 4 24 increase increase NOUN eurjchem-224 4 25 ) ) PUNCT eurjchem-224 4 26     SPACE eurjchem-224 4 27 and and CCONJ eurjchem-224 4 28     SPACE eurjchem-224 4 29 enantiomeric enantiomeric ADJ eurjchem-224 4 30     SPACE eurjchem-224 4 31 excesses excess NOUN eurjchem-224 4 32     SPACE eurjchem-224 4 33 were be AUX eurjchem-224 4 34     SPACE eurjchem-224 4 35 observed observe VERB eurjchem-224 4 36     SPACE eurjchem-224 4 37 in in ADP eurjchem-224 4 38     SPACE eurjchem-224 4 39 each each DET eurjchem-224 4 40     SPACE eurjchem-224 4 41 case case NOUN eurjchem-224 4 42 . . PUNCT eurjchem-224 4 43     SPACE eurjchem-224 4 44 leucine leucine NOUN eurjchem-224 4 45     SPACE eurjchem-224 4 46 valine valine NOUN eurjchem-224 4 47     SPACE eurjchem-224 4 48 enantiomeric enantiomeric ADJ eurjchem-224 4 49     SPACE eurjchem-224 4 50 excess excess ADJ eurjchem-224 4 51     SPACE eurjchem-224 4 52 x‐ray x‐ray ADJ eurjchem-224 4 53     SPACE eurjchem-224 4 54 powder powder NOUN eurjchem-224 4 55     SPACE eurjchem-224 4 56 diffraction diffraction NOUN eurjchem-224 4 57         SPACE eurjchem-224 4 58 1 1 NUM eurjchem-224 4 59 . . PUNCT eurjchem-224 4 60     SPACE eurjchem-224 4 61 introduction introduction NOUN eurjchem-224 4 62         SPACE eurjchem-224 4 63 leucine leucine NOUN eurjchem-224 4 64     SPACE eurjchem-224 5 1 [ [ X eurjchem-224 5 2 1,2 1,2 NUM eurjchem-224 5 3 ] ] PUNCT eurjchem-224 5 4     SPACE eurjchem-224 5 5 and and CCONJ eurjchem-224 5 6     SPACE eurjchem-224 5 7 valine valine NOUN eurjchem-224 5 8     SPACE eurjchem-224 6 1 [ [ X eurjchem-224 6 2 3,4 3,4 NUM eurjchem-224 6 3 ] ] PUNCT eurjchem-224 6 4     SPACE eurjchem-224 6 5 are be AUX eurjchem-224 6 6     SPACE eurjchem-224 6 7 two two NUM eurjchem-224 6 8     SPACE eurjchem-224 6 9 of of ADP eurjchem-224 6 10     SPACE eurjchem-224 6 11 the the DET eurjchem-224 6 12     SPACE eurjchem-224 6 13 twenty twenty NUM eurjchem-224 6 14     SPACE eurjchem-224 6 15 most most ADJ eurjchem-224 6 16     SPACE eurjchem-224 6 17 common common ADJ eurjchem-224 6 18     SPACE eurjchem-224 6 19 amino amino NOUN eurjchem-224 6 20     SPACE eurjchem-224 6 21 acids acid NOUN eurjchem-224 6 22     SPACE eurjchem-224 6 23 on on ADP eurjchem-224 6 24     SPACE eurjchem-224 6 25 earth earth NOUN eurjchem-224 6 26 . . PUNCT eurjchem-224 6 27     SPACE eurjchem-224 7 1 only only ADV eurjchem-224 7 2     SPACE eurjchem-224 7 3 their their PRON eurjchem-224 7 4     SPACE eurjchem-224 7 5 l‐enantiomers l‐enantiomer NOUN eurjchem-224 7 6     SPACE eurjchem-224 7 7 appear appear VERB eurjchem-224 7 8     SPACE eurjchem-224 7 9 in in ADP eurjchem-224 7 10     SPACE eurjchem-224 7 11 mammalian mammalian ADJ eurjchem-224 7 12     SPACE eurjchem-224 7 13 proteins protein NOUN eurjchem-224 7 14 . . PUNCT eurjchem-224 7 15     SPACE eurjchem-224 8 1 they they PRON eurjchem-224 8 2     SPACE eurjchem-224 8 3 are be AUX eurjchem-224 8 4     SPACE eurjchem-224 8 5 essential essential ADJ eurjchem-224 8 6     SPACE eurjchem-224 8 7 in in ADP eurjchem-224 8 8     SPACE eurjchem-224 8 9 meta‐ meta‐ NOUN eurjchem-224 8 10 bolism bolism NOUN eurjchem-224 8 11     SPACE eurjchem-224 8 12 and and CCONJ eurjchem-224 8 13     SPACE eurjchem-224 8 14 necessary necessary ADJ eurjchem-224 8 15     SPACE eurjchem-224 8 16 in in ADP eurjchem-224 8 17     SPACE eurjchem-224 8 18 the the DET eurjchem-224 8 19     SPACE eurjchem-224 8 20 diet diet NOUN eurjchem-224 8 21 , , PUNCT eurjchem-224 8 22     SPACE eurjchem-224 8 23 as as SCONJ eurjchem-224 8 24     SPACE eurjchem-224 8 25 the the DET eurjchem-224 8 26     SPACE eurjchem-224 8 27 human human ADJ eurjchem-224 8 28     SPACE eurjchem-224 8 29 body body NOUN eurjchem-224 8 30     SPACE eurjchem-224 8 31 can can AUX eurjchem-224 8 32 not not PART eurjchem-224 8 33     SPACE eurjchem-224 8 34 synthesize synthesize VERB eurjchem-224 8 35     SPACE eurjchem-224 8 36 them they PRON eurjchem-224 8 37     SPACE eurjchem-224 8 38 from from ADP eurjchem-224 8 39     SPACE eurjchem-224 8 40 simpler simple ADJ eurjchem-224 8 41     SPACE eurjchem-224 8 42 metabolites metabolite NOUN eurjchem-224 8 43 . . PUNCT eurjchem-224 8 44       SPACE eurjchem-224 9 1 they they PRON eurjchem-224 9 2     SPACE eurjchem-224 9 3 are be AUX eurjchem-224 9 4     SPACE eurjchem-224 9 5 branched‐ branched‐ VERB eurjchem-224 9 6 chain chain NOUN eurjchem-224 9 7     SPACE eurjchem-224 9 8 amino amino NOUN eurjchem-224 9 9     SPACE eurjchem-224 9 10 acids acid NOUN eurjchem-224 9 11     SPACE eurjchem-224 9 12 ( ( PUNCT eurjchem-224 9 13 bcaa bcaa NOUN eurjchem-224 9 14 ) ) PUNCT eurjchem-224 9 15 . . PUNCT eurjchem-224 9 16     SPACE eurjchem-224 10 1 bcaa bcaa NOUN eurjchem-224 10 2     SPACE eurjchem-224 10 3 help help NOUN eurjchem-224 10 4     SPACE eurjchem-224 10 5 to to PART eurjchem-224 10 6     SPACE eurjchem-224 10 7 maintain maintain VERB eurjchem-224 10 8     SPACE eurjchem-224 10 9 muscle muscle NOUN eurjchem-224 10 10     SPACE eurjchem-224 10 11 tissue tissue NOUN eurjchem-224 10 12     SPACE eurjchem-224 10 13 and and CCONJ eurjchem-224 10 14     SPACE eurjchem-224 10 15 are be AUX eurjchem-224 10 16     SPACE eurjchem-224 10 17 also also ADV eurjchem-224 10 18     SPACE eurjchem-224 10 19 needed need VERB eurjchem-224 10 20     SPACE eurjchem-224 10 21 during during ADP eurjchem-224 10 22     SPACE eurjchem-224 10 23 times time NOUN eurjchem-224 10 24     SPACE eurjchem-224 10 25 of of ADP eurjchem-224 10 26     SPACE eurjchem-224 10 27 physical physical ADJ eurjchem-224 10 28     SPACE eurjchem-224 10 29 stress stress NOUN eurjchem-224 10 30     SPACE eurjchem-224 10 31 and and CCONJ eurjchem-224 10 32     SPACE eurjchem-224 10 33 intense intense ADJ eurjchem-224 10 34     SPACE eurjchem-224 10 35 exercise exercise NOUN eurjchem-224 10 36 . . PUNCT eurjchem-224 10 37     SPACE eurjchem-224 10 38 young young ADJ eurjchem-224 10 39     SPACE eurjchem-224 10 40 adult adult NOUN eurjchem-224 10 41     SPACE eurjchem-224 10 42 humans human NOUN eurjchem-224 10 43     SPACE eurjchem-224 10 44 need need VERB eurjchem-224 10 45     SPACE eurjchem-224 10 46 about about ADV eurjchem-224 10 47     SPACE eurjchem-224 10 48 31 31 NUM eurjchem-224 10 49     SPACE eurjchem-224 10 50 mg mg NOUN eurjchem-224 10 51     SPACE eurjchem-224 10 52 of of ADP eurjchem-224 10 53     SPACE eurjchem-224 10 54 leucine leucine NOUN eurjchem-224 10 55     SPACE eurjchem-224 10 56 and and CCONJ eurjchem-224 10 57     SPACE eurjchem-224 10 58 23 23 NUM eurjchem-224 10 59     SPACE eurjchem-224 10 60 mg mg NOUN eurjchem-224 10 61     SPACE eurjchem-224 10 62 of of ADP eurjchem-224 10 63     SPACE eurjchem-224 10 64 valine valine NOUN eurjchem-224 10 65     SPACE eurjchem-224 10 66 per per ADP eurjchem-224 10 67     SPACE eurjchem-224 10 68 day day NOUN eurjchem-224 10 69     SPACE eurjchem-224 10 70 per per ADP eurjchem-224 10 71     SPACE eurjchem-224 10 72 kilogram kilogram PROPN eurjchem-224 10 73     SPACE eurjchem-224 10 74 of of ADP eurjchem-224 10 75     SPACE eurjchem-224 10 76 body body NOUN eurjchem-224 10 77     SPACE eurjchem-224 10 78 weight weight NOUN eurjchem-224 10 79 . . PUNCT eurjchem-224 10 80     SPACE eurjchem-224 10 81 leucine leucine NOUN eurjchem-224 10 82 , , PUNCT eurjchem-224 10 83     SPACE eurjchem-224 10 84 ( ( PUNCT eurjchem-224 10 85 ch3)2chch2ch(nh2)cooh ch3)2chch2ch(nh2)cooh VERB eurjchem-224 10 86 , , PUNCT eurjchem-224 10 87     SPACE eurjchem-224 10 88 is be AUX eurjchem-224 10 89     SPACE eurjchem-224 10 90 a a DET eurjchem-224 10 91     SPACE eurjchem-224 10 92 hydrophobic hydrophobic NOUN eurjchem-224 10 93     SPACE eurjchem-224 10 94 amino amino NOUN eurjchem-224 10 95     SPACE eurjchem-224 10 96 acid acid NOUN eurjchem-224 10 97     SPACE eurjchem-224 10 98 that that PRON eurjchem-224 10 99     SPACE eurjchem-224 10 100 is be AUX eurjchem-224 10 101     SPACE eurjchem-224 10 102 found find VERB eurjchem-224 10 103     SPACE eurjchem-224 10 104 as as ADP eurjchem-224 10 105     SPACE eurjchem-224 10 106 a a DET eurjchem-224 10 107     SPACE eurjchem-224 10 108 structural structural ADJ eurjchem-224 10 109     SPACE eurjchem-224 10 110 element element NOUN eurjchem-224 10 111     SPACE eurjchem-224 10 112 in in ADP eurjchem-224 10 113     SPACE eurjchem-224 10 114 the the DET eurjchem-224 10 115     SPACE eurjchem-224 10 116 interior interior NOUN eurjchem-224 10 117     SPACE eurjchem-224 10 118 of of ADP eurjchem-224 10 119     SPACE eurjchem-224 10 120 proteins protein NOUN eurjchem-224 10 121     SPACE eurjchem-224 10 122 and and CCONJ eurjchem-224 10 123     SPACE eurjchem-224 10 124 enzymes enzyme NOUN eurjchem-224 10 125 . . PUNCT eurjchem-224 10 126     SPACE eurjchem-224 11 1 it it PRON eurjchem-224 11 2     SPACE eurjchem-224 11 3 was be AUX eurjchem-224 11 4     SPACE eurjchem-224 11 5 isolated isolate VERB eurjchem-224 11 6     SPACE eurjchem-224 11 7 from from ADP eurjchem-224 11 8     SPACE eurjchem-224 11 9 cheese cheese NOUN eurjchem-224 11 10     SPACE eurjchem-224 11 11 in in ADP eurjchem-224 11 12     SPACE eurjchem-224 11 13 an an DET eurjchem-224 11 14     SPACE eurjchem-224 11 15 impure impure NOUN eurjchem-224 11 16     SPACE eurjchem-224 11 17 form form NOUN eurjchem-224 11 18     SPACE eurjchem-224 11 19 in in ADP eurjchem-224 11 20     SPACE eurjchem-224 11 21 1819 1819 NUM eurjchem-224 11 22     SPACE eurjchem-224 11 23 and and CCONJ eurjchem-224 11 24     SPACE eurjchem-224 11 25 from from ADP eurjchem-224 11 26     SPACE eurjchem-224 11 27 wool wool NOUN eurjchem-224 11 28     SPACE eurjchem-224 11 29 in in ADP eurjchem-224 11 30     SPACE eurjchem-224 11 31 the the DET eurjchem-224 11 32     SPACE eurjchem-224 11 33 crystalline crystalline NOUN eurjchem-224 11 34     SPACE eurjchem-224 11 35 state state NOUN eurjchem-224 11 36     SPACE eurjchem-224 11 37 in in ADP eurjchem-224 11 38     SPACE eurjchem-224 11 39 1820 1820 NUM eurjchem-224 11 40 . . PUNCT eurjchem-224 11 41     SPACE eurjchem-224 11 42 leucine leucine NOUN eurjchem-224 11 43     SPACE eurjchem-224 11 44 stimulates stimulates PROPN eurjchem-224 11 45     SPACE eurjchem-224 11 46 muscle muscle NOUN eurjchem-224 11 47     SPACE eurjchem-224 11 48 protein protein NOUN eurjchem-224 11 49     SPACE eurjchem-224 11 50 synthesis synthesis NOUN eurjchem-224 11 51     SPACE eurjchem-224 11 52 and and CCONJ eurjchem-224 11 53     SPACE eurjchem-224 11 54 may may AUX eurjchem-224 11 55     SPACE eurjchem-224 11 56 be be AUX eurjchem-224 11 57     SPACE eurjchem-224 11 58 the the DET eurjchem-224 11 59     SPACE eurjchem-224 11 60 major major ADJ eurjchem-224 11 61     SPACE eurjchem-224 11 62 fuel fuel NOUN eurjchem-224 11 63     SPACE eurjchem-224 11 64 involved involve VERB eurjchem-224 11 65     SPACE eurjchem-224 11 66 in in ADP eurjchem-224 11 67     SPACE eurjchem-224 11 68 anabolic anabolic NOUN eurjchem-224 11 69     SPACE eurjchem-224 11 70 ( ( PUNCT eurjchem-224 11 71 tissue‐building tissue‐building NOUN eurjchem-224 11 72 ) ) PUNCT eurjchem-224 11 73     SPACE eurjchem-224 11 74 reactions reaction NOUN eurjchem-224 11 75 . . PUNCT eurjchem-224 11 76     SPACE eurjchem-224 12 1 it it PRON eurjchem-224 12 2     SPACE eurjchem-224 12 3 helps help VERB eurjchem-224 12 4     SPACE eurjchem-224 12 5 with with ADP eurjchem-224 12 6     SPACE eurjchem-224 12 7 the the DET eurjchem-224 12 8     SPACE eurjchem-224 12 9 regulation regulation NOUN eurjchem-224 12 10     SPACE eurjchem-224 12 11 of of ADP eurjchem-224 12 12     SPACE eurjchem-224 12 13 blood‐sugar blood‐sugar NOUN eurjchem-224 12 14     SPACE eurjchem-224 12 15 level level NOUN eurjchem-224 12 16 , , PUNCT eurjchem-224 12 17     SPACE eurjchem-224 12 18 growth growth NOUN eurjchem-224 12 19     SPACE eurjchem-224 12 20 hormone hormone NOUN eurjchem-224 12 21     SPACE eurjchem-224 12 22 production production NOUN eurjchem-224 12 23 , , PUNCT eurjchem-224 12 24     SPACE eurjchem-224 12 25 wound wound NOUN eurjchem-224 12 26     SPACE eurjchem-224 12 27 healing healing NOUN eurjchem-224 12 28     SPACE eurjchem-224 12 29 and and CCONJ eurjchem-224 12 30     SPACE eurjchem-224 12 31 energy energy NOUN eurjchem-224 12 32     SPACE eurjchem-224 12 33 regulation regulation NOUN eurjchem-224 12 34 . . PUNCT eurjchem-224 12 35     SPACE eurjchem-224 13 1 it it PRON eurjchem-224 13 2     SPACE eurjchem-224 13 3 is be AUX eurjchem-224 13 4     SPACE eurjchem-224 13 5 found find VERB eurjchem-224 13 6     SPACE eurjchem-224 13 7 in in ADP eurjchem-224 13 8     SPACE eurjchem-224 13 9 protein‐containing protein‐containe VERB eurjchem-224 13 10     SPACE eurjchem-224 13 11 foods food NOUN eurjchem-224 13 12 , , PUNCT eurjchem-224 13 13     SPACE eurjchem-224 13 14 brown brown ADJ eurjchem-224 13 15     SPACE eurjchem-224 13 16 rice rice NOUN eurjchem-224 13 17 , , PUNCT eurjchem-224 13 18     SPACE eurjchem-224 13 19 beans bean NOUN eurjchem-224 13 20 , , PUNCT eurjchem-224 13 21     SPACE eurjchem-224 13 22 nuts nut NOUN eurjchem-224 13 23     SPACE eurjchem-224 13 24 and and CCONJ eurjchem-224 13 25     SPACE eurjchem-224 13 26 wheat wheat NOUN eurjchem-224 13 27 . . PUNCT eurjchem-224 13 28     SPACE eurjchem-224 13 29 valine valine NOUN eurjchem-224 13 30 , , PUNCT eurjchem-224 13 31     SPACE eurjchem-224 13 32 ( ( PUNCT eurjchem-224 13 33 ch3)2chch(nh2)cooh ch3)2chch(nh2)cooh PROPN eurjchem-224 13 34 , , PUNCT eurjchem-224 13 35     SPACE eurjchem-224 13 36 was be AUX eurjchem-224 13 37     SPACE eurjchem-224 13 38 first first ADV eurjchem-224 13 39     SPACE eurjchem-224 13 40 isolated isolate VERB eurjchem-224 13 41     SPACE eurjchem-224 13 42 in in ADP eurjchem-224 13 43     SPACE eurjchem-224 13 44 1888 1888 NUM eurjchem-224 13 45     SPACE eurjchem-224 13 46 by by ADP eurjchem-224 13 47     SPACE eurjchem-224 13 48 weyl weyl VERB eurjchem-224 13 49     SPACE eurjchem-224 14 1 [ [ X eurjchem-224 14 2 5 5 NUM eurjchem-224 14 3 ] ] PUNCT eurjchem-224 14 4 . . PUNCT eurjchem-224 14 5     SPACE eurjchem-224 14 6 it it PRON eurjchem-224 14 7     SPACE eurjchem-224 14 8 has have VERB eurjchem-224 14 9     SPACE eurjchem-224 14 10 a a DET eurjchem-224 14 11     SPACE eurjchem-224 14 12 stimulating stimulate VERB eurjchem-224 14 13     SPACE eurjchem-224 14 14 effect effect NOUN eurjchem-224 14 15     SPACE eurjchem-224 14 16 on on ADP eurjchem-224 14 17     SPACE eurjchem-224 14 18 muscle muscle NOUN eurjchem-224 14 19     SPACE eurjchem-224 14 20 metabolism metabolism NOUN eurjchem-224 14 21     SPACE eurjchem-224 14 22 and and CCONJ eurjchem-224 14 23     SPACE eurjchem-224 14 24 is be AUX eurjchem-224 14 25     SPACE eurjchem-224 14 26 needed need VERB eurjchem-224 14 27     SPACE eurjchem-224 14 28 for for ADP eurjchem-224 14 29     SPACE eurjchem-224 14 30 muscle muscle NOUN eurjchem-224 14 31     SPACE eurjchem-224 14 32 metabolism metabolism NOUN eurjchem-224 14 33 , , PUNCT eurjchem-224 14 34     SPACE eurjchem-224 14 35 repair repair NOUN eurjchem-224 14 36     SPACE eurjchem-224 14 37 and and CCONJ eurjchem-224 14 38     SPACE eurjchem-224 14 39 growth growth NOUN eurjchem-224 14 40     SPACE eurjchem-224 14 41 of of ADP eurjchem-224 14 42     SPACE eurjchem-224 14 43 tissue tissue NOUN eurjchem-224 14 44     SPACE eurjchem-224 14 45 and and CCONJ eurjchem-224 14 46     SPACE eurjchem-224 14 47 maintaining maintain VERB eurjchem-224 14 48     SPACE eurjchem-224 14 49 the the DET eurjchem-224 14 50     SPACE eurjchem-224 14 51 nitrogen nitrogen NOUN eurjchem-224 14 52     SPACE eurjchem-224 14 53 balance balance NOUN eurjchem-224 14 54     SPACE eurjchem-224 14 55 in in ADP eurjchem-224 14 56     SPACE eurjchem-224 14 57 the the DET eurjchem-224 14 58     SPACE eurjchem-224 14 59 body body NOUN eurjchem-224 14 60 . . PUNCT eurjchem-224 14 61     SPACE eurjchem-224 15 1 good good ADJ eurjchem-224 15 2     SPACE eurjchem-224 15 3 sources source NOUN eurjchem-224 15 4     SPACE eurjchem-224 15 5 for for ADP eurjchem-224 15 6     SPACE eurjchem-224 15 7 this this DET eurjchem-224 15 8     SPACE eurjchem-224 15 9 amino amino NOUN eurjchem-224 15 10     SPACE eurjchem-224 15 11 acid acid NOUN eurjchem-224 15 12     SPACE eurjchem-224 15 13 are be AUX eurjchem-224 15 14     SPACE eurjchem-224 15 15 dairy dairy NOUN eurjchem-224 15 16     SPACE eurjchem-224 15 17 produce produce NOUN eurjchem-224 15 18 , , PUNCT eurjchem-224 15 19     SPACE eurjchem-224 15 20 meat meat NOUN eurjchem-224 15 21 , , PUNCT eurjchem-224 15 22     SPACE eurjchem-224 15 23 grain grain NOUN eurjchem-224 15 24 , , PUNCT eurjchem-224 15 25     SPACE eurjchem-224 15 26 mushrooms mushroom NOUN eurjchem-224 15 27 , , PUNCT eurjchem-224 15 28     SPACE eurjchem-224 15 29 soy soy NOUN eurjchem-224 15 30     SPACE eurjchem-224 15 31 and and CCONJ eurjchem-224 15 32     SPACE eurjchem-224 15 33 peanuts peanut NOUN eurjchem-224 15 34 . . PUNCT eurjchem-224 15 35     SPACE eurjchem-224 15 36 today today NOUN eurjchem-224 15 37 , , PUNCT eurjchem-224 15 38     SPACE eurjchem-224 15 39 many many ADJ eurjchem-224 15 40     SPACE eurjchem-224 15 41 athletes athlete NOUN eurjchem-224 15 42     SPACE eurjchem-224 15 43 use use NOUN eurjchem-224 15 44     SPACE eurjchem-224 15 45 leucine leucine NOUN eurjchem-224 15 46     SPACE eurjchem-224 15 47 and and CCONJ eurjchem-224 15 48     SPACE eurjchem-224 15 49 valine valine NOUN eurjchem-224 15 50     SPACE eurjchem-224 15 51 in in ADP eurjchem-224 15 52     SPACE eurjchem-224 15 53 the the DET eurjchem-224 15 54     SPACE eurjchem-224 15 55 l‐ l‐ PROPN eurjchem-224 15 56 enantiomeric enantiomeric ADJ eurjchem-224 15 57     SPACE eurjchem-224 15 58 form form NOUN eurjchem-224 15 59     SPACE eurjchem-224 15 60 as as ADP eurjchem-224 15 61     SPACE eurjchem-224 15 62 supplemental supplemental ADJ eurjchem-224 15 63     SPACE eurjchem-224 15 64 nutrients nutrient NOUN eurjchem-224 15 65 , , PUNCT eurjchem-224 15 66     SPACE eurjchem-224 15 67 so so ADV eurjchem-224 15 68     SPACE eurjchem-224 15 69 easy easy ADJ eurjchem-224 15 70     SPACE eurjchem-224 15 71 and and CCONJ eurjchem-224 15 72     SPACE eurjchem-224 15 73 fast fast ADJ eurjchem-224 15 74     SPACE eurjchem-224 15 75 determination determination NOUN eurjchem-224 15 76     SPACE eurjchem-224 15 77 of of ADP eurjchem-224 15 78     SPACE eurjchem-224 15 79 enantiomeric enantiomeric ADJ eurjchem-224 15 80     SPACE eurjchem-224 15 81 excess excess NOUN eurjchem-224 15 82     SPACE eurjchem-224 15 83 ( ( PUNCT eurjchem-224 15 84 ee ee PROPN eurjchem-224 15 85 ) ) PUNCT eurjchem-224 15 86     SPACE eurjchem-224 15 87 of of ADP eurjchem-224 15 88     SPACE eurjchem-224 15 89 these these DET eurjchem-224 15 90     SPACE eurjchem-224 15 91 amino amino NOUN eurjchem-224 15 92     SPACE eurjchem-224 15 93 acids acid NOUN eurjchem-224 15 94     SPACE eurjchem-224 15 95 is be AUX eurjchem-224 15 96     SPACE eurjchem-224 15 97 very very ADV eurjchem-224 15 98     SPACE eurjchem-224 15 99 important important ADJ eurjchem-224 15 100 . . PUNCT eurjchem-224 15 101     SPACE eurjchem-224 16 1 it it PRON eurjchem-224 16 2     SPACE eurjchem-224 16 3 is be AUX eurjchem-224 16 4     SPACE eurjchem-224 16 5 known know VERB eurjchem-224 16 6     SPACE eurjchem-224 16 7 that that SCONJ eurjchem-224 16 8     SPACE eurjchem-224 16 9 two two NUM eurjchem-224 16 10     SPACE eurjchem-224 16 11 enantiomers enantiomer NOUN eurjchem-224 16 12     SPACE eurjchem-224 16 13 give give VERB eurjchem-224 16 14     SPACE eurjchem-224 16 15 different different ADJ eurjchem-224 16 16     SPACE eurjchem-224 16 17 pharmacological pharmacological NOUN eurjchem-224 16 18     SPACE eurjchem-224 16 19 responses response NOUN eurjchem-224 16 20 , , PUNCT eurjchem-224 16 21     SPACE eurjchem-224 16 22 so so ADV eurjchem-224 16 23     SPACE eurjchem-224 16 24 pharmaceutical pharmaceutical NOUN eurjchem-224 16 25     SPACE eurjchem-224 16 26 companies company NOUN eurjchem-224 16 27     SPACE eurjchem-224 16 28 tend tend VERB eurjchem-224 16 29     SPACE eurjchem-224 16 30 to to PART eurjchem-224 16 31     SPACE eurjchem-224 16 32 produce produce VERB eurjchem-224 16 33     SPACE eurjchem-224 16 34 chiral chiral ADJ eurjchem-224 16 35     SPACE eurjchem-224 16 36 drugs drug NOUN eurjchem-224 16 37     SPACE eurjchem-224 16 38 in in ADP eurjchem-224 16 39     SPACE eurjchem-224 16 40 single single ADJ eurjchem-224 16 41     SPACE eurjchem-224 16 42 enantiomeric enantiomeric ADJ eurjchem-224 16 43     SPACE eurjchem-224 16 44 form form NOUN eurjchem-224 16 45     SPACE eurjchem-224 16 46 and and CCONJ eurjchem-224 16 47     SPACE eurjchem-224 16 48 any any DET eurjchem-224 16 49     SPACE eurjchem-224 16 50 new new ADJ eurjchem-224 16 51     SPACE eurjchem-224 16 52 method method NOUN eurjchem-224 16 53     SPACE eurjchem-224 16 54 able able ADJ eurjchem-224 16 55     SPACE eurjchem-224 16 56 to to PART eurjchem-224 16 57     SPACE eurjchem-224 16 58 control control VERB eurjchem-224 16 59     SPACE eurjchem-224 16 60 the the DET eurjchem-224 16 61     SPACE eurjchem-224 16 62 enantiomeric enantiomeric ADJ eurjchem-224 16 63     SPACE eurjchem-224 16 64 purity purity NOUN eurjchem-224 16 65     SPACE eurjchem-224 16 66 is be AUX eurjchem-224 16 67     SPACE eurjchem-224 16 68 strongly strongly ADV eurjchem-224 16 69     SPACE eurjchem-224 16 70 desired desire VERB eurjchem-224 16 71 . . PUNCT eurjchem-224 16 72     SPACE eurjchem-224 17 1 the the DET eurjchem-224 17 2     SPACE eurjchem-224 17 3 x‐ray x‐ray ADJ eurjchem-224 17 4     SPACE eurjchem-224 17 5 powder powder NOUN eurjchem-224 17 6     SPACE eurjchem-224 17 7 diffraction diffraction NOUN eurjchem-224 17 8     SPACE eurjchem-224 17 9 method method NOUN eurjchem-224 17 10     SPACE eurjchem-224 17 11 ( ( PUNCT eurjchem-224 17 12 xrpd xrpd PROPN eurjchem-224 17 13 ) ) PUNCT eurjchem-224 17 14     SPACE eurjchem-224 17 15 is be AUX eurjchem-224 17 16     SPACE eurjchem-224 17 17 successfully successfully ADV eurjchem-224 17 18     SPACE eurjchem-224 17 19 used use VERB eurjchem-224 17 20     SPACE eurjchem-224 17 21 for for ADP eurjchem-224 17 22     SPACE eurjchem-224 17 23 determination determination NOUN eurjchem-224 17 24     SPACE eurjchem-224 17 25 of of ADP eurjchem-224 17 26     SPACE eurjchem-224 17 27 ee ee ADP eurjchem-224 17 28     SPACE eurjchem-224 17 29 of of ADP eurjchem-224 17 30     SPACE eurjchem-224 17 31 pharmaceuticals pharmaceutical NOUN eurjchem-224 17 32     SPACE eurjchem-224 17 33 such such ADJ eurjchem-224 17 34     SPACE eurjchem-224 17 35 as as ADP eurjchem-224 17 36     SPACE eurjchem-224 17 37 ibuprofen ibuprofen NOUN eurjchem-224 17 38     SPACE eurjchem-224 17 39 ( ( PUNCT eurjchem-224 17 40 anti‐inflammatory anti‐inflammatory PROPN eurjchem-224 17 41 , , PUNCT eurjchem-224 17 42     SPACE eurjchem-224 17 43 analgesic analgesic ADJ eurjchem-224 17 44     SPACE eurjchem-224 17 45 and and CCONJ eurjchem-224 17 46     SPACE eurjchem-224 17 47 antipyretic antipyretic ADJ eurjchem-224 17 48     SPACE eurjchem-224 17 49 agent agent NOUN eurjchem-224 17 50     SPACE eurjchem-224 18 1 [ [ X eurjchem-224 18 2 6,7 6,7 NUM eurjchem-224 18 3 ] ] PUNCT eurjchem-224 18 4 ) ) PUNCT eurjchem-224 18 5     SPACE eurjchem-224 19 1 [ [ X eurjchem-224 19 2 8 8 NUM eurjchem-224 19 3 ] ] SYM eurjchem-224 19 4     SPACE eurjchem-224 19 5 and and CCONJ eurjchem-224 19 6     SPACE eurjchem-224 19 7 cyclophosph cyclophosph NOUN eurjchem-224 19 8     SPACE eurjchem-224 19 9 amide amide NOUN eurjchem-224 19 10     SPACE eurjchem-224 19 11 ( ( PUNCT eurjchem-224 19 12 anticancer anticancer NOUN eurjchem-224 19 13     SPACE eurjchem-224 19 14 agent agent NOUN eurjchem-224 19 15     SPACE eurjchem-224 19 16 [ [ X eurjchem-224 19 17 9‐11 9‐11 NUM eurjchem-224 19 18 ] ] NOUN eurjchem-224 19 19 ) ) PUNCT eurjchem-224 19 20     SPACE eurjchem-224 19 21 [ [ X eurjchem-224 19 22 12 12 NUM eurjchem-224 19 23 ] ] PUNCT eurjchem-224 19 24 . . PUNCT eurjchem-224 19 25     SPACE eurjchem-224 19 26 now now ADV eurjchem-224 19 27     SPACE eurjchem-224 19 28 extension extension NOUN eurjchem-224 19 29     SPACE eurjchem-224 19 30 of of ADP eurjchem-224 19 31     SPACE eurjchem-224 19 32 the the DET eurjchem-224 19 33     SPACE eurjchem-224 19 34 xrpd xrpd ADJ eurjchem-224 19 35     SPACE eurjchem-224 19 36 technique technique NOUN eurjchem-224 19 37     SPACE eurjchem-224 19 38 to to ADP eurjchem-224 19 39     SPACE eurjchem-224 19 40 the the DET eurjchem-224 19 41     SPACE eurjchem-224 19 42 determination determination NOUN eurjchem-224 19 43     SPACE eurjchem-224 19 44 of of ADP eurjchem-224 19 45     SPACE eurjchem-224 19 46 enantiomeric enantiomeric ADJ eurjchem-224 19 47     SPACE eurjchem-224 19 48 excess excess NOUN eurjchem-224 19 49     SPACE eurjchem-224 19 50 in in ADP eurjchem-224 19 51     SPACE eurjchem-224 19 52 the the DET eurjchem-224 19 53     SPACE eurjchem-224 19 54 mixtures mixture NOUN eurjchem-224 19 55     SPACE eurjchem-224 19 56 of of ADP eurjchem-224 19 57     SPACE eurjchem-224 19 58 leucine leucine NOUN eurjchem-224 19 59     SPACE eurjchem-224 19 60 or or CCONJ eurjchem-224 19 61     SPACE eurjchem-224 19 62 valine valine NOUN eurjchem-224 19 63     SPACE eurjchem-224 19 64 is be AUX eurjchem-224 19 65     SPACE eurjchem-224 19 66 presented present VERB eurjchem-224 19 67 . . PUNCT eurjchem-224 19 68         SPACE eurjchem-224 20 1 2 2 NUM eurjchem-224 20 2 . . PUNCT eurjchem-224 20 3     SPACE eurjchem-224 20 4 experimental experimental ADJ eurjchem-224 20 5         SPACE eurjchem-224 20 6 the the DET eurjchem-224 20 7     SPACE eurjchem-224 20 8 samples sample NOUN eurjchem-224 20 9     SPACE eurjchem-224 20 10 of of ADP eurjchem-224 20 11     SPACE eurjchem-224 20 12 racemeric racemeric NOUN eurjchem-224 20 13     SPACE eurjchem-224 20 14 ( ( PUNCT eurjchem-224 20 15 dl dl NOUN eurjchem-224 20 16 ) ) PUNCT eurjchem-224 20 17     SPACE eurjchem-224 20 18 and and CCONJ eurjchem-224 20 19     SPACE eurjchem-224 20 20 enantiomeric enantiomeric NOUN eurjchem-224 20 21     SPACE eurjchem-224 20 22 ( ( PUNCT eurjchem-224 20 23 l l NOUN eurjchem-224 20 24 ) ) PUNCT eurjchem-224 20 25     SPACE eurjchem-224 20 26 leucine leucine NOUN eurjchem-224 20 27     SPACE eurjchem-224 20 28 were be AUX eurjchem-224 20 29     SPACE eurjchem-224 20 30 mixed mixed ADJ eurjchem-224 20 31     SPACE eurjchem-224 20 32 in in ADP eurjchem-224 20 33     SPACE eurjchem-224 20 34 different different ADJ eurjchem-224 20 35     SPACE eurjchem-224 20 36 proportions proportion NOUN eurjchem-224 20 37     SPACE eurjchem-224 20 38 to to PART eurjchem-224 20 39     SPACE eurjchem-224 20 40 prepare prepare VERB eurjchem-224 20 41     SPACE eurjchem-224 20 42 physical physical ADJ eurjchem-224 20 43     SPACE eurjchem-224 20 44 mixtures mixture NOUN eurjchem-224 20 45 . . PUNCT eurjchem-224 20 46     SPACE eurjchem-224 21 1 the the DET eurjchem-224 21 2     SPACE eurjchem-224 21 3 ee ee NOUN eurjchem-224 21 4     SPACE eurjchem-224 21 5 values value NOUN eurjchem-224 21 6     SPACE eurjchem-224 21 7 were be AUX eurjchem-224 21 8     SPACE eurjchem-224 21 9 5 5 NUM eurjchem-224 21 10 % % NOUN eurjchem-224 21 11 , , PUNCT eurjchem-224 21 12     SPACE eurjchem-224 21 13 10 10 NUM eurjchem-224 21 14 % % NOUN eurjchem-224 21 15 , , PUNCT eurjchem-224 21 16     SPACE eurjchem-224 21 17 25 25 NUM eurjchem-224 21 18 % % NOUN eurjchem-224 21 19 , , PUNCT eurjchem-224 21 20     SPACE eurjchem-224 21 21 40 40 NUM eurjchem-224 21 22 % % NOUN eurjchem-224 21 23 , , PUNCT eurjchem-224 21 24     SPACE eurjchem-224 21 25 50 50 NUM eurjchem-224 21 26 % % NOUN eurjchem-224 21 27 , , PUNCT eurjchem-224 21 28     SPACE eurjchem-224 21 29 60 60 NUM eurjchem-224 21 30 % % NOUN eurjchem-224 21 31 , , PUNCT eurjchem-224 21 32     SPACE eurjchem-224 21 33 75 75 NUM eurjchem-224 21 34 % % NOUN eurjchem-224 21 35 , , PUNCT eurjchem-224 21 36     SPACE eurjchem-224 21 37 90 90 NUM eurjchem-224 21 38 % % NOUN eurjchem-224 21 39 . . PUNCT eurjchem-224 21 40     SPACE eurjchem-224 22 1 analogous analogous ADJ eurjchem-224 22 2     SPACE eurjchem-224 22 3 samples sample NOUN eurjchem-224 22 4     SPACE eurjchem-224 22 5 were be AUX eurjchem-224 22 6     SPACE eurjchem-224 22 7 prepared prepare VERB eurjchem-224 22 8     SPACE eurjchem-224 22 9 for for ADP eurjchem-224 22 10     SPACE eurjchem-224 22 11 valine valine NOUN eurjchem-224 22 12 . . PUNCT eurjchem-224 22 13         SPACE eurjchem-224 23 1 the the DET eurjchem-224 23 2     SPACE eurjchem-224 23 3 physical physical ADJ eurjchem-224 23 4     SPACE eurjchem-224 23 5 mixtures mixture NOUN eurjchem-224 23 6     SPACE eurjchem-224 23 7 and and CCONJ eurjchem-224 23 8     SPACE eurjchem-224 23 9 recrystallized recrystallize VERB eurjchem-224 23 10     SPACE eurjchem-224 23 11 physical physical ADJ eurjchem-224 23 12     SPACE eurjchem-224 23 13 mixtures mixture NOUN eurjchem-224 23 14     SPACE eurjchem-224 23 15 ( ( PUNCT eurjchem-224 23 16 meoh meoh PROPN eurjchem-224 23 17 : : PUNCT eurjchem-224 23 18 h2o h2o PROPN eurjchem-224 23 19 , , PUNCT eurjchem-224 23 20     SPACE eurjchem-224 23 21 1:1 1:1 NUM eurjchem-224 23 22 ) ) PUNCT eurjchem-224 23 23     SPACE eurjchem-224 23 24 of of ADP eurjchem-224 23 25     SPACE eurjchem-224 23 26 these these DET eurjchem-224 23 27     SPACE eurjchem-224 23 28 amino amino NOUN eurjchem-224 23 29     SPACE eurjchem-224 23 30 acids acid NOUN eurjchem-224 23 31     SPACE eurjchem-224 23 32 were be AUX eurjchem-224 23 33     SPACE eurjchem-224 23 34 prepared prepare VERB eurjchem-224 23 35 . . PUNCT eurjchem-224 23 36     SPACE eurjchem-224 23 37 recrystallized recrystallize VERB eurjchem-224 23 38     SPACE eurjchem-224 23 39 physical physical ADJ eurjchem-224 23 40     SPACE eurjchem-224 23 41 mixtures mixture NOUN eurjchem-224 23 42     SPACE eurjchem-224 23 43 were be AUX eurjchem-224 23 44     SPACE eurjchem-224 23 45 prepared prepare VERB eurjchem-224 23 46     SPACE eurjchem-224 23 47 in in ADP eurjchem-224 23 48     SPACE eurjchem-224 23 49 different different ADJ eurjchem-224 23 50     SPACE eurjchem-224 23 51 ways way NOUN eurjchem-224 23 52 : : PUNCT eurjchem-224 23 53     SPACE eurjchem-224 23 54 slow slow ADJ eurjchem-224 23 55     SPACE eurjchem-224 23 56 evaporation evaporation NOUN eurjchem-224 23 57     SPACE eurjchem-224 23 58 techniques technique NOUN eurjchem-224 23 59     SPACE eurjchem-224 23 60 and and CCONJ eurjchem-224 23 61     SPACE eurjchem-224 23 62 fast fast ADJ eurjchem-224 23 63     SPACE eurjchem-224 23 64 evaporation evaporation NOUN eurjchem-224 23 65     SPACE eurjchem-224 23 66 in in ADP eurjchem-224 23 67     SPACE eurjchem-224 23 68 a a DET eurjchem-224 23 69     SPACE eurjchem-224 23 70 rotary rotary NOUN eurjchem-224 23 71     SPACE eurjchem-224 23 72 evaporator evaporator NOUN eurjchem-224 23 73     SPACE eurjchem-224 23 74 ( ( PUNCT eurjchem-224 23 75 pressure pressure NOUN eurjchem-224 23 76     SPACE eurjchem-224 23 77 100 100 NUM eurjchem-224 23 78     SPACE eurjchem-224 23 79 mm mm PROPN eurjchem-224 23 80     SPACE eurjchem-224 23 81 hg hg NOUN eurjchem-224 23 82 , , PUNCT eurjchem-224 23 83     SPACE eurjchem-224 23 84 temperature temperature NOUN eurjchem-224 23 85 : : PUNCT eurjchem-224 23 86     SPACE eurjchem-224 23 87 19 19 NUM eurjchem-224 23 88     SPACE eurjchem-224 23 89 ° ° NOUN eurjchem-224 23 90 c c NOUN eurjchem-224 23 91 ; ; PUNCT eurjchem-224 23 92     SPACE eurjchem-224 23 93 pressure pressure NOUN eurjchem-224 23 94 : : PUNCT eurjchem-224 23 95     SPACE eurjchem-224 23 96 500 500 NUM eurjchem-224 23 97     SPACE eurjchem-224 23 98 mmhg mmhg NOUN eurjchem-224 23 99 , , PUNCT eurjchem-224 23 100     SPACE eurjchem-224 23 101 temperature temperature NOUN eurjchem-224 23 102 : : PUNCT eurjchem-224 23 103     SPACE eurjchem-224 23 104 40 40 NUM eurjchem-224 23 105     SPACE eurjchem-224 23 106 ° ° NOUN eurjchem-224 23 107 c c NOUN eurjchem-224 23 108 ) ) PUNCT eurjchem-224 23 109 . . PUNCT eurjchem-224 23 110     SPACE eurjchem-224 24 1 in in ADP eurjchem-224 24 2     SPACE eurjchem-224 24 3 all all DET eurjchem-224 24 4     SPACE eurjchem-224 24 5 cases case NOUN eurjchem-224 24 6     SPACE eurjchem-224 24 7 the the DET eurjchem-224 24 8     SPACE eurjchem-224 24 9 same same ADJ eurjchem-224 24 10     SPACE eurjchem-224 24 11 mixtures mixture NOUN eurjchem-224 24 12     SPACE eurjchem-224 24 13 recrystallized recrystallize VERB eurjchem-224 24 14     SPACE eurjchem-224 24 15 by by ADP eurjchem-224 24 16     SPACE eurjchem-224 24 17 different different ADJ eurjchem-224 24 18     SPACE eurjchem-224 24 19 methods method NOUN eurjchem-224 24 20     SPACE eurjchem-224 24 21 gave give VERB eurjchem-224 24 22     SPACE eurjchem-224 24 23 identical identical ADJ eurjchem-224 24 24     SPACE eurjchem-224 24 25 diffraction diffraction NOUN eurjchem-224 24 26     SPACE eurjchem-224 24 27 patterns pattern NOUN eurjchem-224 24 28 , , PUNCT eurjchem-224 24 29     SPACE eurjchem-224 24 30 i.e. i.e. X eurjchem-224 24 31     SPACE eurjchem-224 24 32 the the DET eurjchem-224 24 33     SPACE eurjchem-224 24 34 peaks peak NOUN eurjchem-224 24 35     SPACE eurjchem-224 24 36 have have VERB eurjchem-224 24 37     SPACE eurjchem-224 24 38 the the DET eurjchem-224 24 39     SPACE eurjchem-224 24 40 same same ADJ eurjchem-224 24 41     SPACE eurjchem-224 24 42 positions position NOUN eurjchem-224 24 43     SPACE eurjchem-224 24 44 and and CCONJ eurjchem-224 24 45     SPACE eurjchem-224 24 46 intensities intensity NOUN eurjchem-224 24 47 . . PUNCT eurjchem-224 24 48     SPACE eurjchem-224 24 49 to to PART eurjchem-224 24 50     SPACE eurjchem-224 24 51 avoid avoid VERB eurjchem-224 24 52     SPACE eurjchem-224 24 53 errors error NOUN eurjchem-224 24 54     SPACE eurjchem-224 24 55 associated associate VERB eurjchem-224 24 56     SPACE eurjchem-224 24 57 with with ADP eurjchem-224 24 58     SPACE eurjchem-224 24 59 change change NOUN eurjchem-224 24 60     SPACE eurjchem-224 24 61 of of ADP eurjchem-224 24 62     SPACE eurjchem-224 24 63 ee ee NOUN eurjchem-224 24 64     SPACE eurjchem-224 24 65 during during ADP eurjchem-224 24 66     SPACE eurjchem-224 24 67 the the DET eurjchem-224 24 68     SPACE eurjchem-224 24 69 recrystallization recrystallization NOUN eurjchem-224 24 70     SPACE eurjchem-224 24 71 the the DET eurjchem-224 24 72     SPACE eurjchem-224 24 73 ee ee NOUN eurjchem-224 24 74     SPACE eurjchem-224 24 75 was be AUX eurjchem-224 24 76     SPACE eurjchem-224 24 77 monitored monitor VERB eurjchem-224 24 78     SPACE eurjchem-224 24 79 also also ADV eurjchem-224 24 80     SPACE eurjchem-224 24 81 by by ADP eurjchem-224 24 82     SPACE eurjchem-224 24 83 13c 13c NOUN eurjchem-224 24 84     SPACE eurjchem-224 24 85 cp cp PROPN eurjchem-224 24 86 / / SYM eurjchem-224 24 87 mas mas PROPN eurjchem-224 24 88     SPACE eurjchem-224 24 89 and and CCONJ eurjchem-224 24 90     SPACE eurjchem-224 24 91 odessa odessa ADJ eurjchem-224 24 92     SPACE eurjchem-224 24 93 nmr nmr NOUN eurjchem-224 24 94     SPACE eurjchem-224 24 95 experiments experiment NOUN eurjchem-224 24 96 . . PUNCT eurjchem-224 24 97         SPACE eurjchem-224 24 98 2.1 2.1 NUM eurjchem-224 24 99 . . PUNCT eurjchem-224 24 100     SPACE eurjchem-224 24 101 instrumentation instrumentation NOUN eurjchem-224 24 102         SPACE eurjchem-224 24 103 the the DET eurjchem-224 24 104     SPACE eurjchem-224 24 105 substances substance NOUN eurjchem-224 24 106     SPACE eurjchem-224 24 107 and and CCONJ eurjchem-224 24 108     SPACE eurjchem-224 24 109 mixtures mixture NOUN eurjchem-224 24 110     SPACE eurjchem-224 24 111 discussed discuss VERB eurjchem-224 24 112     SPACE eurjchem-224 24 113 above above ADP eurjchem-224 24 114     SPACE eurjchem-224 24 115 were be AUX eurjchem-224 24 116     SPACE eurjchem-224 24 117 milled mill VERB eurjchem-224 24 118     SPACE eurjchem-224 24 119 in in ADP eurjchem-224 24 120     SPACE eurjchem-224 24 121 the the DET eurjchem-224 24 122     SPACE eurjchem-224 24 123 planetary planetary ADJ eurjchem-224 24 124     SPACE eurjchem-224 24 125 ball ball NOUN eurjchem-224 24 126     SPACE eurjchem-224 24 127 corundum corundum NOUN eurjchem-224 24 128     SPACE eurjchem-224 24 129 mill mill NOUN eurjchem-224 24 130     SPACE eurjchem-224 24 131 for for ADP eurjchem-224 24 132     SPACE eurjchem-224 24 133 5 5 NUM eurjchem-224 24 134     SPACE eurjchem-224 24 135 minutes minute NOUN eurjchem-224 24 136     SPACE eurjchem-224 24 137 and and CCONJ eurjchem-224 24 138     SPACE eurjchem-224 24 139 the the DET eurjchem-224 24 140     SPACE eurjchem-224 24 141 x‐ray x‐ray NOUN eurjchem-224 24 142     SPACE eurjchem-224 24 143 diffractograms diffractogram NOUN eurjchem-224 24 144     SPACE eurjchem-224 24 145 were be AUX eurjchem-224 24 146     SPACE eurjchem-224 24 147 then then ADV eurjchem-224 24 148     SPACE eurjchem-224 24 149 recorded record VERB eurjchem-224 24 150     SPACE eurjchem-224 24 151 using use VERB eurjchem-224 24 152     SPACE eurjchem-224 24 153 a a DET eurjchem-224 24 154     SPACE eurjchem-224 24 155 d‐5000 d‐5000 NOUN eurjchem-224 24 156     SPACE eurjchem-224 24 157 diffractometer diffractometer NOUN eurjchem-224 24 158     SPACE eurjchem-224 24 159 and and CCONJ eurjchem-224 24 160     SPACE eurjchem-224 24 161 cukα cukα NOUN eurjchem-224 24 162     SPACE eurjchem-224 24 163 ( ( PUNCT eurjchem-224 24 164 ni‐filtered ni‐filtere VERB eurjchem-224 24 165 ) ) PUNCT eurjchem-224 24 166     SPACE eurjchem-224 24 167 radiation radiation NOUN eurjchem-224 24 168     SPACE eurjchem-224 24 169 with with ADP eurjchem-224 24 170     SPACE eurjchem-224 24 171 bragg‐ bragg‐ PROPN eurjchem-224 24 172 320 320 NUM eurjchem-224 24 173     SPACE eurjchem-224 24 174 tadeusiak tadeusiak NOUN eurjchem-224 24 175     SPACE eurjchem-224 24 176 et et PROPN eurjchem-224 24 177     SPACE eurjchem-224 24 178 al al PROPN eurjchem-224 24 179 . . PROPN eurjchem-224 24 180     SPACE eurjchem-224 24 181 / / SYM eurjchem-224 24 182     SPACE eurjchem-224 24 183 european european ADJ eurjchem-224 24 184     SPACE eurjchem-224 24 185 journal journal NOUN eurjchem-224 24 186     SPACE eurjchem-224 24 187 of of ADP eurjchem-224 24 188     SPACE eurjchem-224 24 189 chemistry chemistry NOUN eurjchem-224 24 190     SPACE eurjchem-224 24 191 1 1 NUM eurjchem-224 24 192     SPACE eurjchem-224 24 193 ( ( PUNCT eurjchem-224 24 194 4 4 NUM eurjchem-224 24 195 ) ) PUNCT eurjchem-224 24 196     SPACE eurjchem-224 24 197 ( ( PUNCT eurjchem-224 24 198 2010 2010 NUM eurjchem-224 24 199 ) ) PUNCT eurjchem-224 24 200     SPACE eurjchem-224 25 1 319­321 319­321 NUM eurjchem-224 25 2         SPACE eurjchem-224 25 3 brentano brentano VERB eurjchem-224 25 4     SPACE eurjchem-224 25 5 focusing focus VERB eurjchem-224 25 6     SPACE eurjchem-224 25 7 geometry geometry NOUN eurjchem-224 25 8 . . PUNCT eurjchem-224 25 9     SPACE eurjchem-224 26 1 the the DET eurjchem-224 26 2     SPACE eurjchem-224 26 3 measurements measurement NOUN eurjchem-224 26 4     SPACE eurjchem-224 26 5 were be AUX eurjchem-224 26 6     SPACE eurjchem-224 26 7 made make VERB eurjchem-224 26 8     SPACE eurjchem-224 26 9 in in ADP eurjchem-224 26 10     SPACE eurjchem-224 26 11 the the DET eurjchem-224 26 12     SPACE eurjchem-224 26 13 2θ 2θ NUM eurjchem-224 26 14     SPACE eurjchem-224 27 1 = = NOUN eurjchem-224 27 2     SPACE eurjchem-224 27 3 2‐80 2‐80 NUM eurjchem-224 27 4 ° ° NOUN eurjchem-224 27 5     SPACE eurjchem-224 27 6 range range NOUN eurjchem-224 27 7     SPACE eurjchem-224 27 8 with with ADP eurjchem-224 27 9     SPACE eurjchem-224 27 10 2 2 NUM eurjchem-224 27 11     SPACE eurjchem-224 27 12 seconds second NOUN eurjchem-224 27 13     SPACE eurjchem-224 27 14 per per ADP eurjchem-224 27 15     SPACE eurjchem-224 27 16 0.01 0.01 NUM eurjchem-224 27 17 ° ° NOUN eurjchem-224 27 18     SPACE eurjchem-224 27 19 step step NOUN eurjchem-224 27 20 . . PUNCT eurjchem-224 27 21     SPACE eurjchem-224 28 1 the the DET eurjchem-224 28 2     SPACE eurjchem-224 28 3 area area NOUN eurjchem-224 28 4     SPACE eurjchem-224 28 5 of of ADP eurjchem-224 28 6     SPACE eurjchem-224 28 7 peak peak NOUN eurjchem-224 28 8     SPACE eurjchem-224 28 9 was be AUX eurjchem-224 28 10     SPACE eurjchem-224 28 11 computed compute VERB eurjchem-224 28 12     SPACE eurjchem-224 28 13 by by ADP eurjchem-224 28 14     SPACE eurjchem-224 28 15 eva eva PROPN eurjchem-224 28 16     SPACE eurjchem-224 28 17 version version NOUN eurjchem-224 28 18     SPACE eurjchem-224 28 19 3.09 3.09 NUM eurjchem-224 28 20     SPACE eurjchem-224 28 21 from from ADP eurjchem-224 28 22     SPACE eurjchem-224 28 23 diffrac diffrac NOUN eurjchem-224 28 24     SPACE eurjchem-224 28 25 at at ADP eurjchem-224 28 26     SPACE eurjchem-224 28 27 program program NOUN eurjchem-224 28 28     SPACE eurjchem-224 28 29 package package NOUN eurjchem-224 28 30     SPACE eurjchem-224 28 31 with with ADP eurjchem-224 28 32     SPACE eurjchem-224 28 33 ω‐2θ ω‐2θ ADV eurjchem-224 28 34     SPACE eurjchem-224 28 35 scan scan ADJ eurjchem-224 28 36     SPACE eurjchem-224 28 37 mode mode NOUN eurjchem-224 28 38     SPACE eurjchem-224 28 39 after after ADP eurjchem-224 28 40     SPACE eurjchem-224 28 41 appropriate appropriate ADJ eurjchem-224 28 42     SPACE eurjchem-224 28 43 background background NOUN eurjchem-224 28 44     SPACE eurjchem-224 28 45 determination determination NOUN eurjchem-224 28 46     SPACE eurjchem-224 29 1 [ [ X eurjchem-224 29 2 13 13 NUM eurjchem-224 29 3 ] ] PUNCT eurjchem-224 29 4 . . PUNCT eurjchem-224 29 5         SPACE eurjchem-224 30 1 3 3 NUM eurjchem-224 30 2 . . PUNCT eurjchem-224 30 3     SPACE eurjchem-224 30 4 results result VERB eurjchem-224 30 5     SPACE eurjchem-224 30 6 and and CCONJ eurjchem-224 30 7     SPACE eurjchem-224 30 8 discussion discussion NOUN eurjchem-224 30 9         SPACE eurjchem-224 30 10 the the DET eurjchem-224 30 11     SPACE eurjchem-224 30 12 structures structure NOUN eurjchem-224 30 13     SPACE eurjchem-224 30 14 of of ADP eurjchem-224 30 15     SPACE eurjchem-224 30 16 l‐leucine l‐leucine NOUN eurjchem-224 30 17     SPACE eurjchem-224 31 1 [ [ X eurjchem-224 31 2 14‐16 14‐16 NUM eurjchem-224 31 3 ] ] X eurjchem-224 31 4     SPACE eurjchem-224 31 5 / / SYM eurjchem-224 31 6     SPACE eurjchem-224 31 7 l‐valine l‐valine NOUN eurjchem-224 31 8     SPACE eurjchem-224 31 9 [ [ X eurjchem-224 31 10 17‐19 17‐19 NUM eurjchem-224 31 11 ] ] SYM eurjchem-224 31 12     SPACE eurjchem-224 31 13 and and CCONJ eurjchem-224 31 14     SPACE eurjchem-224 31 15 their their PRON eurjchem-224 31 16     SPACE eurjchem-224 31 17 racemates racemate NOUN eurjchem-224 31 18     SPACE eurjchem-224 31 19 ( ( PUNCT eurjchem-224 31 20 dl‐leucine dl‐leucine NOUN eurjchem-224 31 21     SPACE eurjchem-224 31 22 [ [ X eurjchem-224 31 23 20,21 20,21 NUM eurjchem-224 31 24 ] ] SYM eurjchem-224 31 25     SPACE eurjchem-224 31 26 / / SYM eurjchem-224 31 27     SPACE eurjchem-224 31 28 dl‐valine dl‐valine NOUN eurjchem-224 31 29     SPACE eurjchem-224 31 30 [ [ X eurjchem-224 31 31 22‐25 22‐25 NOUN eurjchem-224 31 32 ] ] PUNCT eurjchem-224 31 33 ) ) PUNCT eurjchem-224 31 34     SPACE eurjchem-224 31 35 are be AUX eurjchem-224 31 36     SPACE eurjchem-224 31 37 different different ADJ eurjchem-224 31 38     SPACE eurjchem-224 31 39 ( ( PUNCT eurjchem-224 31 40 for for SCONJ eurjchem-224 31 41     SPACE eurjchem-224 31 42 details detail NOUN eurjchem-224 31 43     SPACE eurjchem-224 31 44 see see VERB eurjchem-224 31 45     SPACE eurjchem-224 31 46 supplementary supplementary ADJ eurjchem-224 31 47     SPACE eurjchem-224 31 48 materials material NOUN eurjchem-224 31 49 ) ) PUNCT eurjchem-224 31 50 , , PUNCT eurjchem-224 31 51     SPACE eurjchem-224 31 52 which which PRON eurjchem-224 31 53     SPACE eurjchem-224 31 54 result result VERB eurjchem-224 31 55     SPACE eurjchem-224 31 56 in in ADP eurjchem-224 31 57     SPACE eurjchem-224 31 58 different different ADJ eurjchem-224 31 59     SPACE eurjchem-224 31 60 powder powder NOUN eurjchem-224 31 61     SPACE eurjchem-224 31 62 patterns pattern NOUN eurjchem-224 31 63 . . PUNCT eurjchem-224 31 64     SPACE eurjchem-224 32 1 this this PRON eurjchem-224 32 2     SPACE eurjchem-224 32 3 allows allow VERB eurjchem-224 32 4     SPACE eurjchem-224 32 5 both both DET eurjchem-224 32 6     SPACE eurjchem-224 32 7 phase phase NOUN eurjchem-224 32 8     SPACE eurjchem-224 32 9 identification identification NOUN eurjchem-224 32 10     SPACE eurjchem-224 32 11 and and CCONJ eurjchem-224 32 12     SPACE eurjchem-224 32 13 quantitative quantitative ADJ eurjchem-224 32 14     SPACE eurjchem-224 32 15 analysis analysis NOUN eurjchem-224 32 16 . . PUNCT eurjchem-224 32 17     SPACE eurjchem-224 33 1 recorded record VERB eurjchem-224 33 2     SPACE eurjchem-224 33 3 diffractograms diffractogram NOUN eurjchem-224 33 4     SPACE eurjchem-224 33 5 of of ADP eurjchem-224 33 6     SPACE eurjchem-224 33 7 the the DET eurjchem-224 33 8     SPACE eurjchem-224 33 9 pure pure ADJ eurjchem-224 33 10     SPACE eurjchem-224 33 11 amino amino NOUN eurjchem-224 33 12     SPACE eurjchem-224 33 13 acids acid NOUN eurjchem-224 33 14 , , PUNCT eurjchem-224 33 15     SPACE eurjchem-224 33 16 leucine leucine NOUN eurjchem-224 33 17     SPACE eurjchem-224 33 18 and and CCONJ eurjchem-224 33 19     SPACE eurjchem-224 33 20 valine valine NOUN eurjchem-224 33 21     SPACE eurjchem-224 33 22 in in ADP eurjchem-224 33 23     SPACE eurjchem-224 33 24 racemic racemic NOUN eurjchem-224 33 25     SPACE eurjchem-224 33 26 and and CCONJ eurjchem-224 33 27     SPACE eurjchem-224 33 28 enantiomeric enantiomeric ADJ eurjchem-224 33 29     SPACE eurjchem-224 33 30 forms form NOUN eurjchem-224 33 31 , , PUNCT eurjchem-224 33 32     SPACE eurjchem-224 33 33 are be AUX eurjchem-224 33 34     SPACE eurjchem-224 33 35 depicted depict VERB eurjchem-224 33 36     SPACE eurjchem-224 33 37 in in ADP eurjchem-224 33 38     SPACE eurjchem-224 33 39 figure figure NOUN eurjchem-224 33 40     SPACE eurjchem-224 33 41 1 1 NUM eurjchem-224 33 42     SPACE eurjchem-224 33 43 and and CCONJ eurjchem-224 33 44     SPACE eurjchem-224 33 45 2 2 NUM eurjchem-224 33 46 . . PUNCT eurjchem-224 33 47     SPACE eurjchem-224 33 48 the the DET eurjchem-224 33 49     SPACE eurjchem-224 33 50 sample sample NOUN eurjchem-224 33 51     SPACE eurjchem-224 33 52 x‐ray x‐ray ADJ eurjchem-224 33 53     SPACE eurjchem-224 33 54 powder powder NOUN eurjchem-224 33 55     SPACE eurjchem-224 33 56 diffraction diffraction NOUN eurjchem-224 33 57     SPACE eurjchem-224 33 58 patterns pattern NOUN eurjchem-224 33 59     SPACE eurjchem-224 33 60 of of ADP eurjchem-224 33 61     SPACE eurjchem-224 33 62 prepared prepared ADJ eurjchem-224 33 63     SPACE eurjchem-224 33 64 mixtures mixture NOUN eurjchem-224 33 65     SPACE eurjchem-224 33 66 are be AUX eurjchem-224 33 67     SPACE eurjchem-224 33 68 depicted depict VERB eurjchem-224 33 69     SPACE eurjchem-224 33 70 on on ADP eurjchem-224 33 71     SPACE eurjchem-224 33 72 figure figure NOUN eurjchem-224 33 73     SPACE eurjchem-224 33 74 3 3 NUM eurjchem-224 33 75     SPACE eurjchem-224 33 76 and and CCONJ eurjchem-224 33 77     SPACE eurjchem-224 33 78 4 4 NUM eurjchem-224 33 79 . . PUNCT eurjchem-224 33 80             SPACE eurjchem-224 34 1 ( ( PUNCT eurjchem-224 34 2 a a X eurjchem-224 34 3 ) ) PUNCT eurjchem-224 34 4     SPACE eurjchem-224 34 5 ( ( PUNCT eurjchem-224 34 6 b b NOUN eurjchem-224 34 7 ) ) PUNCT eurjchem-224 34 8         SPACE eurjchem-224 34 9 figure figure NOUN eurjchem-224 34 10     SPACE eurjchem-224 34 11 1 1 NUM eurjchem-224 34 12 . . PUNCT eurjchem-224 34 13     SPACE eurjchem-224 34 14 diffractogram diffractogram PROPN eurjchem-224 34 15     SPACE eurjchem-224 34 16 of of ADP eurjchem-224 34 17     SPACE eurjchem-224 34 18 ( ( PUNCT eurjchem-224 34 19 a a PRON eurjchem-224 34 20 ) ) PUNCT eurjchem-224 34 21     SPACE eurjchem-224 34 22 leucine leucine NOUN eurjchem-224 34 23     SPACE eurjchem-224 34 24 ( ( PUNCT eurjchem-224 34 25 racemate racemate ADJ eurjchem-224 34 26 ) ) PUNCT eurjchem-224 34 27 , , PUNCT eurjchem-224 34 28     SPACE eurjchem-224 34 29 ( ( PUNCT eurjchem-224 34 30 b b NOUN eurjchem-224 34 31 ) ) PUNCT eurjchem-224 34 32     SPACE eurjchem-224 34 33 leucine leucine NOUN eurjchem-224 34 34     SPACE eurjchem-224 34 35 ( ( PUNCT eurjchem-224 34 36 l‐enantiomer l‐enantiomer NUM eurjchem-224 34 37 ) ) PUNCT eurjchem-224 34 38 . . PUNCT eurjchem-224 34 39         SPACE eurjchem-224 35 1 ( ( PUNCT eurjchem-224 35 2 a a X eurjchem-224 35 3 ) ) PUNCT eurjchem-224 35 4     SPACE eurjchem-224 35 5 ( ( PUNCT eurjchem-224 35 6 b b NOUN eurjchem-224 35 7 ) ) PUNCT eurjchem-224 35 8         SPACE eurjchem-224 35 9 figure figure NOUN eurjchem-224 35 10     SPACE eurjchem-224 35 11 2 2 NUM eurjchem-224 35 12 . . PUNCT eurjchem-224 35 13     SPACE eurjchem-224 35 14 diffractogram diffractogram PROPN eurjchem-224 35 15     SPACE eurjchem-224 35 16 of of ADP eurjchem-224 35 17     SPACE eurjchem-224 35 18 ( ( PUNCT eurjchem-224 35 19 a a PRON eurjchem-224 35 20 ) ) PUNCT eurjchem-224 35 21     SPACE eurjchem-224 35 22 valine valine NOUN eurjchem-224 35 23 : : PUNCT eurjchem-224 35 24     SPACE eurjchem-224 35 25 racemate racemate VERB eurjchem-224 35 26 , , PUNCT eurjchem-224 35 27     SPACE eurjchem-224 35 28 ( ( PUNCT eurjchem-224 35 29 b b NOUN eurjchem-224 35 30 ) ) PUNCT eurjchem-224 35 31     SPACE eurjchem-224 35 32 valine valine NOUN eurjchem-224 35 33 : : PUNCT eurjchem-224 35 34     SPACE eurjchem-224 35 35 l‐enantiomer l‐enantiomer X eurjchem-224 35 36 . . PUNCT eurjchem-224 36 1 ( ( PUNCT eurjchem-224 36 2 a a X eurjchem-224 36 3 ) ) PUNCT eurjchem-224 36 4     SPACE eurjchem-224 36 5 ( ( PUNCT eurjchem-224 36 6 b b NOUN eurjchem-224 36 7 ) ) PUNCT eurjchem-224 36 8         SPACE eurjchem-224 36 9 figure figure NOUN eurjchem-224 36 10     SPACE eurjchem-224 36 11 3 3 NUM eurjchem-224 36 12 . . PUNCT eurjchem-224 36 13     SPACE eurjchem-224 36 14 diffractogram diffractogram PROPN eurjchem-224 36 15     SPACE eurjchem-224 36 16 of of ADP eurjchem-224 36 17     SPACE eurjchem-224 36 18 leucine leucine NOUN eurjchem-224 36 19     SPACE eurjchem-224 36 20 ( ( PUNCT eurjchem-224 36 21 ee ee NOUN eurjchem-224 36 22     SPACE eurjchem-224 36 23 = = NOUN eurjchem-224 36 24     SPACE eurjchem-224 36 25 75 75 NUM eurjchem-224 36 26 % % NOUN eurjchem-224 36 27 ) ) PUNCT eurjchem-224 36 28     SPACE eurjchem-224 36 29 ( ( PUNCT eurjchem-224 36 30 a a X eurjchem-224 36 31 ) ) PUNCT eurjchem-224 36 32     SPACE eurjchem-224 36 33 physical physical ADJ eurjchem-224 36 34     SPACE eurjchem-224 36 35 mixture mixture NOUN eurjchem-224 36 36 . . PUNCT eurjchem-224 36 37     SPACE eurjchem-224 37 1 ( ( PUNCT eurjchem-224 37 2 b b X eurjchem-224 37 3 ) ) PUNCT eurjchem-224 37 4     SPACE eurjchem-224 37 5 recrystallized recrystallize VERB eurjchem-224 37 6     SPACE eurjchem-224 37 7 mixture mixture NOUN eurjchem-224 37 8 . . PUNCT eurjchem-224 37 9     SPACE eurjchem-224 38 1 ( ( PUNCT eurjchem-224 38 2 a a X eurjchem-224 38 3 ) ) PUNCT eurjchem-224 38 4     SPACE eurjchem-224 38 5 ( ( PUNCT eurjchem-224 38 6 b b NOUN eurjchem-224 38 7 ) ) PUNCT eurjchem-224 38 8         SPACE eurjchem-224 38 9 figure figure NOUN eurjchem-224 38 10     SPACE eurjchem-224 38 11 4 4 NUM eurjchem-224 38 12 . . PUNCT eurjchem-224 38 13     SPACE eurjchem-224 38 14 diffractogram diffractogram PROPN eurjchem-224 38 15     SPACE eurjchem-224 38 16 of of ADP eurjchem-224 38 17     SPACE eurjchem-224 38 18 valine valine NOUN eurjchem-224 38 19     SPACE eurjchem-224 38 20 ( ( PUNCT eurjchem-224 38 21 ee ee ADP eurjchem-224 38 22     SPACE eurjchem-224 38 23 = = VERB eurjchem-224 38 24     SPACE eurjchem-224 38 25 25 25 NUM eurjchem-224 38 26 % % NOUN eurjchem-224 38 27 ) ) PUNCT eurjchem-224 38 28     SPACE eurjchem-224 38 29 ( ( PUNCT eurjchem-224 38 30 a a X eurjchem-224 38 31 ) ) PUNCT eurjchem-224 38 32     SPACE eurjchem-224 38 33 physical physical ADJ eurjchem-224 38 34     SPACE eurjchem-224 38 35 mixture mixture NOUN eurjchem-224 38 36 , , PUNCT eurjchem-224 38 37     SPACE eurjchem-224 38 38 ( ( PUNCT eurjchem-224 38 39 b b NOUN eurjchem-224 38 40 ) ) PUNCT eurjchem-224 38 41     SPACE eurjchem-224 38 42 recrystallized recrystallize VERB eurjchem-224 38 43     SPACE eurjchem-224 38 44 mixture mixture NOUN eurjchem-224 38 45 . . PUNCT eurjchem-224 38 46         SPACE eurjchem-224 38 47 for for ADP eurjchem-224 38 48     SPACE eurjchem-224 38 49 each each DET eurjchem-224 38 50     SPACE eurjchem-224 38 51 pattern pattern NOUN eurjchem-224 38 52     SPACE eurjchem-224 38 53 one one NUM eurjchem-224 38 54     SPACE eurjchem-224 38 55 non‐overlapping non‐overlappe VERB eurjchem-224 38 56     SPACE eurjchem-224 38 57 independent independent ADJ eurjchem-224 38 58     SPACE eurjchem-224 38 59 diffraction diffraction NOUN eurjchem-224 38 60     SPACE eurjchem-224 38 61 peak peak NOUN eurjchem-224 38 62     SPACE eurjchem-224 38 63 for for ADP eurjchem-224 38 64     SPACE eurjchem-224 38 65 the the DET eurjchem-224 38 66     SPACE eurjchem-224 38 67 l‐amino l‐amino NOUN eurjchem-224 38 68     SPACE eurjchem-224 38 69 acid acid NOUN eurjchem-224 38 70     SPACE eurjchem-224 38 71 and and CCONJ eurjchem-224 38 72     SPACE eurjchem-224 38 73 the the DET eurjchem-224 38 74     SPACE eurjchem-224 38 75 racemate racemate NOUN eurjchem-224 38 76     SPACE eurjchem-224 38 77 can can AUX eurjchem-224 38 78     SPACE eurjchem-224 38 79 be be AUX eurjchem-224 38 80     SPACE eurjchem-224 38 81 selected select VERB eurjchem-224 38 82     SPACE eurjchem-224 38 83 ( ( PUNCT eurjchem-224 38 84 for for ADP eurjchem-224 38 85     SPACE eurjchem-224 38 86 the the DET eurjchem-224 38 87     SPACE eurjchem-224 38 88 leucine leucine NOUN eurjchem-224 38 89     SPACE eurjchem-224 38 90 l‐enantiomer l‐enantiomer AUX eurjchem-224 38 91     SPACE eurjchem-224 38 92 at at ADP eurjchem-224 38 93     SPACE eurjchem-224 38 94 2θ 2θ NUM eurjchem-224 38 95     SPACE eurjchem-224 39 1 = = NOUN eurjchem-224 39 2     SPACE eurjchem-224 39 3 24.3 24.3 NUM eurjchem-224 39 4 ° ° NOUN eurjchem-224 39 5     SPACE eurjchem-224 39 6 and and CCONJ eurjchem-224 39 7     SPACE eurjchem-224 39 8 for for ADP eurjchem-224 39 9     SPACE eurjchem-224 39 10 the the DET eurjchem-224 39 11     SPACE eurjchem-224 39 12 leucine leucine NOUN eurjchem-224 39 13     SPACE eurjchem-224 39 14 racemate racemate VERB eurjchem-224 39 15     SPACE eurjchem-224 39 16 at at ADP eurjchem-224 39 17     SPACE eurjchem-224 39 18 2θ 2θ NUM eurjchem-224 39 19     SPACE eurjchem-224 39 20 = = NOUN eurjchem-224 39 21     SPACE eurjchem-224 39 22 25.3 25.3 NUM eurjchem-224 39 23 ° ° NOUN eurjchem-224 39 24 ; ; PUNCT eurjchem-224 39 25     SPACE eurjchem-224 39 26 and and CCONJ eurjchem-224 39 27     SPACE eurjchem-224 39 28 for for ADP eurjchem-224 39 29     SPACE eurjchem-224 39 30 valine valine NOUN eurjchem-224 39 31     SPACE eurjchem-224 39 32 at at ADP eurjchem-224 39 33     SPACE eurjchem-224 39 34 29.5 29.5 NUM eurjchem-224 39 35 ° ° NUM eurjchem-224 39 36     SPACE eurjchem-224 39 37 and and CCONJ eurjchem-224 39 38     SPACE eurjchem-224 39 39 32.4 32.4 NUM eurjchem-224 39 40 ° ° NOUN eurjchem-224 39 41     SPACE eurjchem-224 39 42 for for ADP eurjchem-224 39 43     SPACE eurjchem-224 39 44 the the DET eurjchem-224 39 45     SPACE eurjchem-224 39 46 l‐enantiomer l‐enantiomer NUM eurjchem-224 39 47     SPACE eurjchem-224 39 48 and and CCONJ eurjchem-224 39 49     SPACE eurjchem-224 39 50 racemate racemate VERB eurjchem-224 39 51 , , PUNCT eurjchem-224 39 52     SPACE eurjchem-224 39 53 respectively respectively ADV eurjchem-224 39 54 ) ) PUNCT eurjchem-224 39 55 . . PUNCT eurjchem-224 39 56     SPACE eurjchem-224 40 1 thus thus ADV eurjchem-224 40 2     SPACE eurjchem-224 40 3 the the DET eurjchem-224 40 4     SPACE eurjchem-224 40 5 classic classic ADJ eurjchem-224 40 6     SPACE eurjchem-224 40 7 approach approach NOUN eurjchem-224 40 8     SPACE eurjchem-224 40 9 based base VERB eurjchem-224 40 10     SPACE eurjchem-224 40 11 on on ADP eurjchem-224 40 12     SPACE eurjchem-224 40 13 the the DET eurjchem-224 40 14     SPACE eurjchem-224 40 15 intensity intensity NOUN eurjchem-224 40 16     SPACE eurjchem-224 40 17 of of ADP eurjchem-224 40 18     SPACE eurjchem-224 40 19 one one NUM eurjchem-224 40 20     SPACE eurjchem-224 40 21 peak peak NOUN eurjchem-224 40 22     SPACE eurjchem-224 40 23 can can AUX eurjchem-224 40 24     SPACE eurjchem-224 40 25 be be AUX eurjchem-224 40 26     SPACE eurjchem-224 40 27 applied apply VERB eurjchem-224 40 28     SPACE eurjchem-224 40 29 instead instead ADV eurjchem-224 40 30     SPACE eurjchem-224 40 31 of of ADP eurjchem-224 40 32     SPACE eurjchem-224 40 33 the the DET eurjchem-224 40 34     SPACE eurjchem-224 40 35 rieteveld rieteveld VERB eurjchem-224 40 36     SPACE eurjchem-224 40 37 method method NOUN eurjchem-224 40 38 . . PUNCT eurjchem-224 40 39     SPACE eurjchem-224 41 1 fitting fit VERB eurjchem-224 41 2     SPACE eurjchem-224 41 3 the the DET eurjchem-224 41 4     SPACE eurjchem-224 41 5 whole whole ADJ eurjchem-224 41 6     SPACE eurjchem-224 41 7 diffraction diffraction NOUN eurjchem-224 41 8     SPACE eurjchem-224 41 9 pattern pattern NOUN eurjchem-224 41 10     SPACE eurjchem-224 41 11 to to ADP eurjchem-224 41 12     SPACE eurjchem-224 41 13 the the DET eurjchem-224 41 14     SPACE eurjchem-224 41 15 calculated calculate VERB eurjchem-224 41 16     SPACE eurjchem-224 41 17 intensities intensity NOUN eurjchem-224 41 18     SPACE eurjchem-224 41 19 for for ADP eurjchem-224 41 20     SPACE eurjchem-224 41 21 the the DET eurjchem-224 41 22     SPACE eurjchem-224 41 23 various various ADJ eurjchem-224 41 24     SPACE eurjchem-224 41 25 phases phase NOUN eurjchem-224 41 26     SPACE eurjchem-224 41 27 that that PRON eurjchem-224 41 28     SPACE eurjchem-224 41 29 are be AUX eurjchem-224 41 30     SPACE eurjchem-224 41 31 present present ADJ eurjchem-224 41 32     SPACE eurjchem-224 41 33 can can AUX eurjchem-224 41 34     SPACE eurjchem-224 41 35 give give VERB eurjchem-224 41 36     SPACE eurjchem-224 41 37 more more ADJ eurjchem-224 41 38     SPACE eurjchem-224 41 39 precise precise ADJ eurjchem-224 41 40     SPACE eurjchem-224 41 41 results result NOUN eurjchem-224 41 42 , , PUNCT eurjchem-224 41 43     SPACE eurjchem-224 41 44 but but CCONJ eurjchem-224 41 45     SPACE eurjchem-224 41 46 in in ADP eurjchem-224 41 47     SPACE eurjchem-224 41 48 the the DET eurjchem-224 41 49     SPACE eurjchem-224 41 50 case case NOUN eurjchem-224 41 51     SPACE eurjchem-224 41 52 discussed discuss VERB eurjchem-224 41 53     SPACE eurjchem-224 41 54 here here ADV eurjchem-224 41 55     SPACE eurjchem-224 41 56 the the DET eurjchem-224 41 57     SPACE eurjchem-224 41 58 classic classic ADJ eurjchem-224 41 59     SPACE eurjchem-224 41 60 approach approach NOUN eurjchem-224 41 61     SPACE eurjchem-224 41 62 gives give VERB eurjchem-224 41 63     SPACE eurjchem-224 41 64 a a DET eurjchem-224 41 65     SPACE eurjchem-224 41 66 linear linear ADJ eurjchem-224 41 67     SPACE eurjchem-224 41 68 correlation correlation NOUN eurjchem-224 41 69     SPACE eurjchem-224 41 70 between between ADP eurjchem-224 41 71     SPACE eurjchem-224 41 72 the the DET eurjchem-224 41 73     SPACE eurjchem-224 41 74 intensity intensity NOUN eurjchem-224 41 75     SPACE eurjchem-224 41 76 ( ( PUNCT eurjchem-224 41 77 the the DET eurjchem-224 41 78     SPACE eurjchem-224 41 79 area area NOUN eurjchem-224 41 80     SPACE eurjchem-224 41 81 of of ADP eurjchem-224 41 82     SPACE eurjchem-224 41 83 the the DET eurjchem-224 41 84     SPACE eurjchem-224 41 85 peak peak NOUN eurjchem-224 41 86 ) ) PUNCT eurjchem-224 41 87     SPACE eurjchem-224 41 88 and and CCONJ eurjchem-224 41 89     SPACE eurjchem-224 41 90 the the DET eurjchem-224 41 91     SPACE eurjchem-224 41 92 ee ee NOUN eurjchem-224 41 93     SPACE eurjchem-224 41 94 in in ADP eurjchem-224 41 95     SPACE eurjchem-224 41 96 each each DET eurjchem-224 41 97     SPACE eurjchem-224 41 98 cases case NOUN eurjchem-224 41 99     SPACE eurjchem-224 41 100 ( ( PUNCT eurjchem-224 41 101 figure figure NOUN eurjchem-224 41 102     SPACE eurjchem-224 41 103 5 5 NUM eurjchem-224 41 104     SPACE eurjchem-224 41 105 and and CCONJ eurjchem-224 41 106     SPACE eurjchem-224 41 107 figure figure NOUN eurjchem-224 41 108     SPACE eurjchem-224 41 109 6 6 NUM eurjchem-224 41 110 ) ) PUNCT eurjchem-224 41 111     SPACE eurjchem-224 41 112 with with ADP eurjchem-224 41 113     SPACE eurjchem-224 41 114 r2 r2 PROPN eurjchem-224 41 115     SPACE eurjchem-224 41 116 values value NOUN eurjchem-224 41 117     SPACE eurjchem-224 41 118 greater great ADJ eurjchem-224 41 119     SPACE eurjchem-224 41 120 than than ADP eurjchem-224 41 121     SPACE eurjchem-224 41 122 0.99 0.99 NUM eurjchem-224 41 123 . . PUNCT eurjchem-224 41 124     SPACE eurjchem-224 41 125 tadeusiak tadeusiak PROPN eurjchem-224 41 126     SPACE eurjchem-224 41 127 et et PROPN eurjchem-224 41 128     SPACE eurjchem-224 41 129 al al PROPN eurjchem-224 41 130 . . PROPN eurjchem-224 41 131     SPACE eurjchem-224 41 132 / / SYM eurjchem-224 41 133     SPACE eurjchem-224 41 134 european european ADJ eurjchem-224 41 135     SPACE eurjchem-224 41 136 journal journal NOUN eurjchem-224 41 137     SPACE eurjchem-224 41 138 of of ADP eurjchem-224 41 139     SPACE eurjchem-224 41 140 chemistry chemistry NOUN eurjchem-224 41 141     SPACE eurjchem-224 41 142 1 1 NUM eurjchem-224 41 143     SPACE eurjchem-224 41 144 ( ( PUNCT eurjchem-224 41 145 4 4 NUM eurjchem-224 41 146 ) ) PUNCT eurjchem-224 41 147     SPACE eurjchem-224 41 148 ( ( PUNCT eurjchem-224 41 149 2010 2010 NUM eurjchem-224 41 150 ) ) PUNCT eurjchem-224 41 151     SPACE eurjchem-224 41 152 319­321 319­321 NUM eurjchem-224 41 153     SPACE eurjchem-224 41 154 321 321 NUM eurjchem-224 41 155         SPACE eurjchem-224 41 156 ( ( PUNCT eurjchem-224 41 157 a a NOUN eurjchem-224 41 158 ) ) PUNCT eurjchem-224 41 159             SPACE eurjchem-224 41 160 ( ( PUNCT eurjchem-224 41 161 b b NOUN eurjchem-224 41 162 ) ) PUNCT eurjchem-224 41 163         SPACE eurjchem-224 41 164 figure figure NOUN eurjchem-224 41 165     SPACE eurjchem-224 41 166 5 5 NUM eurjchem-224 41 167 . . PUNCT eurjchem-224 41 168     SPACE eurjchem-224 41 169 linear linear ADJ eurjchem-224 41 170     SPACE eurjchem-224 41 171 correlation correlation NOUN eurjchem-224 41 172     SPACE eurjchem-224 41 173 between between ADP eurjchem-224 41 174     SPACE eurjchem-224 41 175 intensity intensity NOUN eurjchem-224 41 176     SPACE eurjchem-224 41 177 and and CCONJ eurjchem-224 41 178     SPACE eurjchem-224 41 179 ee ee NOUN eurjchem-224 41 180     SPACE eurjchem-224 41 181 in in ADP eurjchem-224 41 182     SPACE eurjchem-224 41 183 samples sample NOUN eurjchem-224 41 184     SPACE eurjchem-224 41 185 of of ADP eurjchem-224 41 186     SPACE eurjchem-224 41 187 leucine leucine NOUN eurjchem-224 41 188     SPACE eurjchem-224 41 189 ( ( PUNCT eurjchem-224 41 190 physical physical ADJ eurjchem-224 41 191     SPACE eurjchem-224 41 192 mixture mixture NOUN eurjchem-224 41 193 ) ) PUNCT eurjchem-224 41 194     SPACE eurjchem-224 41 195 – – PUNCT eurjchem-224 41 196     SPACE eurjchem-224 41 197 reflection reflection NOUN eurjchem-224 41 198 : : PUNCT eurjchem-224 41 199     SPACE eurjchem-224 41 200 2θ 2θ NUM eurjchem-224 41 201     SPACE eurjchem-224 42 1 = = NOUN eurjchem-224 42 2     SPACE eurjchem-224 42 3 24.3˚ 24.3˚ NOUN eurjchem-224 42 4     SPACE eurjchem-224 42 5 ( ( PUNCT eurjchem-224 42 6 enantiomer enantiomer NOUN eurjchem-224 42 7 ) ) PUNCT eurjchem-224 42 8 ; ; PUNCT eurjchem-224 42 9     SPACE eurjchem-224 42 10 reflection reflection NOUN eurjchem-224 42 11 : : PUNCT eurjchem-224 42 12     SPACE eurjchem-224 42 13 2θ 2θ NUM eurjchem-224 42 14     SPACE eurjchem-224 42 15 = = NOUN eurjchem-224 42 16     SPACE eurjchem-224 42 17 25.3˚ 25.3˚ NOUN eurjchem-224 42 18     SPACE eurjchem-224 42 19 ( ( PUNCT eurjchem-224 42 20 racemate racemate ADJ eurjchem-224 42 21 ) ) PUNCT eurjchem-224 42 22     SPACE eurjchem-224 42 23 ( ( PUNCT eurjchem-224 42 24 a a X eurjchem-224 42 25 ) ) PUNCT eurjchem-224 42 26     SPACE eurjchem-224 42 27 physical physical ADJ eurjchem-224 42 28     SPACE eurjchem-224 42 29 mixture mixture NOUN eurjchem-224 42 30 , , PUNCT eurjchem-224 42 31     SPACE eurjchem-224 42 32 ( ( PUNCT eurjchem-224 42 33 b b NOUN eurjchem-224 42 34 ) ) PUNCT eurjchem-224 42 35     SPACE eurjchem-224 42 36 recrystallized recrystallize VERB eurjchem-224 42 37     SPACE eurjchem-224 42 38 mixture mixture NOUN eurjchem-224 42 39 . . PUNCT eurjchem-224 42 40         SPACE eurjchem-224 43 1 ( ( PUNCT eurjchem-224 43 2 a a X eurjchem-224 43 3 ) ) PUNCT eurjchem-224 43 4         SPACE eurjchem-224 43 5 ( ( PUNCT eurjchem-224 43 6 b b NOUN eurjchem-224 43 7 ) ) PUNCT eurjchem-224 43 8         SPACE eurjchem-224 43 9 figure figure NOUN eurjchem-224 43 10     SPACE eurjchem-224 43 11 6 6 NUM eurjchem-224 43 12 . . PUNCT eurjchem-224 43 13     SPACE eurjchem-224 43 14 linear linear ADJ eurjchem-224 43 15     SPACE eurjchem-224 43 16 correlation correlation NOUN eurjchem-224 43 17     SPACE eurjchem-224 43 18 between between ADP eurjchem-224 43 19     SPACE eurjchem-224 43 20 intensity intensity NOUN eurjchem-224 43 21     SPACE eurjchem-224 43 22 and and CCONJ eurjchem-224 43 23     SPACE eurjchem-224 43 24 ee ee NOUN eurjchem-224 43 25     SPACE eurjchem-224 43 26 in in ADP eurjchem-224 43 27     SPACE eurjchem-224 43 28 samples sample NOUN eurjchem-224 43 29     SPACE eurjchem-224 43 30 of of ADP eurjchem-224 43 31     SPACE eurjchem-224 43 32 valine valine NOUN eurjchem-224 43 33     SPACE eurjchem-224 43 34 ( ( PUNCT eurjchem-224 43 35 physical physical ADJ eurjchem-224 43 36     SPACE eurjchem-224 43 37 mixture mixture NOUN eurjchem-224 43 38 ) ) PUNCT eurjchem-224 43 39     SPACE eurjchem-224 43 40 – – PUNCT eurjchem-224 43 41     SPACE eurjchem-224 43 42 reflection reflection NOUN eurjchem-224 43 43 : : PUNCT eurjchem-224 43 44     SPACE eurjchem-224 43 45 2θ 2θ NUM eurjchem-224 43 46     SPACE eurjchem-224 43 47 = = NOUN eurjchem-224 43 48     SPACE eurjchem-224 43 49 32.4˚(enantiomer 32.4˚(enantiomer NUM eurjchem-224 43 50 ) ) PUNCT eurjchem-224 43 51 ; ; PUNCT eurjchem-224 43 52     SPACE eurjchem-224 43 53 reflection reflection NOUN eurjchem-224 43 54 : : PUNCT eurjchem-224 43 55     SPACE eurjchem-224 43 56 2θ 2θ NUM eurjchem-224 43 57     SPACE eurjchem-224 44 1 = = NOUN eurjchem-224 44 2     SPACE eurjchem-224 44 3 29.5˚ 29.5˚ NOUN eurjchem-224 44 4     SPACE eurjchem-224 44 5 ( ( PUNCT eurjchem-224 44 6 racemate racemate ADJ eurjchem-224 44 7 ) ) PUNCT eurjchem-224 44 8     SPACE eurjchem-224 44 9 ( ( PUNCT eurjchem-224 44 10 a a X eurjchem-224 44 11 ) ) PUNCT eurjchem-224 44 12     SPACE eurjchem-224 44 13 physical physical ADJ eurjchem-224 44 14     SPACE eurjchem-224 44 15 mixture mixture NOUN eurjchem-224 44 16     SPACE eurjchem-224 44 17 ( ( PUNCT eurjchem-224 44 18 b b NOUN eurjchem-224 44 19 ) ) PUNCT eurjchem-224 44 20     SPACE eurjchem-224 44 21 recrystallized recrystallize VERB eurjchem-224 44 22     SPACE eurjchem-224 44 23 mixture mixture NOUN eurjchem-224 44 24 . . PUNCT eurjchem-224 44 25         SPACE eurjchem-224 45 1 as as SCONJ eurjchem-224 45 2     SPACE eurjchem-224 45 3 it it PRON eurjchem-224 45 4     SPACE eurjchem-224 45 5 is be AUX eurjchem-224 45 6     SPACE eurjchem-224 45 7 shown show VERB eurjchem-224 45 8     SPACE eurjchem-224 45 9 in in ADP eurjchem-224 45 10     SPACE eurjchem-224 45 11 figure figure NOUN eurjchem-224 45 12     SPACE eurjchem-224 45 13 5 5 NUM eurjchem-224 45 14     SPACE eurjchem-224 45 15 and and CCONJ eurjchem-224 45 16     SPACE eurjchem-224 45 17 figure figure NOUN eurjchem-224 45 18     SPACE eurjchem-224 45 19 6 6 NUM eurjchem-224 45 20     SPACE eurjchem-224 45 21 the the DET eurjchem-224 45 22     SPACE eurjchem-224 45 23 regression regression NOUN eurjchem-224 45 24     SPACE eurjchem-224 45 25 coefficients coefficient NOUN eurjchem-224 45 26     SPACE eurjchem-224 45 27 differ differ VERB eurjchem-224 45 28     SPACE eurjchem-224 45 29 for for ADP eurjchem-224 45 30     SPACE eurjchem-224 45 31 physical physical ADJ eurjchem-224 45 32     SPACE eurjchem-224 45 33 mixtures mixture NOUN eurjchem-224 45 34     SPACE eurjchem-224 45 35 and and CCONJ eurjchem-224 45 36     SPACE eurjchem-224 45 37 recrystallised recrystallise VERB eurjchem-224 45 38     SPACE eurjchem-224 45 39 samples sample NOUN eurjchem-224 45 40 . . PUNCT eurjchem-224 45 41     SPACE eurjchem-224 46 1 it it PRON eurjchem-224 46 2     SPACE eurjchem-224 46 3 is be AUX eurjchem-224 46 4     SPACE eurjchem-224 46 5 caused cause VERB eurjchem-224 46 6     SPACE eurjchem-224 46 7 by by ADP eurjchem-224 46 8     SPACE eurjchem-224 46 9 differences difference NOUN eurjchem-224 46 10     SPACE eurjchem-224 46 11 in in ADP eurjchem-224 46 12     SPACE eurjchem-224 46 13 the the DET eurjchem-224 46 14     SPACE eurjchem-224 46 15 degree degree NOUN eurjchem-224 46 16     SPACE eurjchem-224 46 17 of of ADP eurjchem-224 46 18     SPACE eurjchem-224 46 19 crystallinity crystallinity NOUN eurjchem-224 46 20     SPACE eurjchem-224 46 21 of of ADP eurjchem-224 46 22     SPACE eurjchem-224 46 23 determined determine VERB eurjchem-224 46 24     SPACE eurjchem-224 46 25 compounds compound NOUN eurjchem-224 46 26 . . PUNCT eurjchem-224 46 27     SPACE eurjchem-224 47 1 thus thus ADV eurjchem-224 47 2     SPACE eurjchem-224 47 3 all all DET eurjchem-224 47 4     SPACE eurjchem-224 47 5 standard standard NOUN eurjchem-224 47 6     SPACE eurjchem-224 47 7 samples sample NOUN eurjchem-224 47 8     SPACE eurjchem-224 47 9 must must AUX eurjchem-224 47 10     SPACE eurjchem-224 47 11 be be AUX eurjchem-224 47 12     SPACE eurjchem-224 47 13 recrystallised recrystallise VERB eurjchem-224 47 14     SPACE eurjchem-224 47 15 to to PART eurjchem-224 47 16     SPACE eurjchem-224 47 17 obtain obtain VERB eurjchem-224 47 18     SPACE eurjchem-224 47 19 reliable reliable ADJ eurjchem-224 47 20     SPACE eurjchem-224 47 21 results result NOUN eurjchem-224 47 22 . . PUNCT eurjchem-224 47 23     SPACE eurjchem-224 48 1 prepared prepare VERB eurjchem-224 48 2     SPACE eurjchem-224 48 3 physical physical ADJ eurjchem-224 48 4     SPACE eurjchem-224 48 5 mixtures mixture NOUN eurjchem-224 48 6     SPACE eurjchem-224 48 7 diffractograms diffractogram NOUN eurjchem-224 48 8     SPACE eurjchem-224 48 9 did do AUX eurjchem-224 48 10     SPACE eurjchem-224 48 11 not not PART eurjchem-224 48 12     SPACE eurjchem-224 48 13 show show VERB eurjchem-224 48 14     SPACE eurjchem-224 48 15 a a DET eurjchem-224 48 16     SPACE eurjchem-224 48 17 dependence dependence NOUN eurjchem-224 48 18     SPACE eurjchem-224 48 19 on on ADP eurjchem-224 48 20     SPACE eurjchem-224 48 21 method method NOUN eurjchem-224 48 22     SPACE eurjchem-224 48 23 of of ADP eurjchem-224 48 24     SPACE eurjchem-224 48 25 preparation preparation NOUN eurjchem-224 48 26     SPACE eurjchem-224 48 27 ‐ ‐ VERB eurjchem-224 48 28     SPACE eurjchem-224 48 29 slow slow ADJ eurjchem-224 48 30     SPACE eurjchem-224 48 31 evaporation evaporation NOUN eurjchem-224 48 32     SPACE eurjchem-224 48 33 or or CCONJ eurjchem-224 48 34     SPACE eurjchem-224 48 35 fast fast ADJ eurjchem-224 48 36     SPACE eurjchem-224 48 37 evaporation evaporation NOUN eurjchem-224 48 38     SPACE eurjchem-224 48 39 in in ADP eurjchem-224 48 40     SPACE eurjchem-224 48 41 a a DET eurjchem-224 48 42     SPACE eurjchem-224 48 43 rotary rotary NOUN eurjchem-224 48 44     SPACE eurjchem-224 48 45 evaporator evaporator NOUN eurjchem-224 48 46     SPACE eurjchem-224 48 47 ( ( PUNCT eurjchem-224 48 48 pressure pressure NOUN eurjchem-224 48 49 : : PUNCT eurjchem-224 48 50     SPACE eurjchem-224 48 51 100 100 NUM eurjchem-224 48 52     SPACE eurjchem-224 48 53 mm mm PROPN eurjchem-224 48 54     SPACE eurjchem-224 48 55 hg hg NOUN eurjchem-224 48 56 , , PUNCT eurjchem-224 48 57     SPACE eurjchem-224 48 58 temperature temperature NOUN eurjchem-224 48 59 : : PUNCT eurjchem-224 48 60     SPACE eurjchem-224 48 61 19 19 NUM eurjchem-224 48 62     SPACE eurjchem-224 48 63 ° ° NOUN eurjchem-224 48 64 c c NOUN eurjchem-224 48 65 ; ; PUNCT eurjchem-224 48 66     SPACE eurjchem-224 48 67 pressure pressure NOUN eurjchem-224 48 68 : : PUNCT eurjchem-224 48 69     SPACE eurjchem-224 48 70 500 500 NUM eurjchem-224 48 71     SPACE eurjchem-224 48 72 mmhg mmhg NOUN eurjchem-224 48 73 , , PUNCT eurjchem-224 48 74     SPACE eurjchem-224 48 75 temperature temperature NOUN eurjchem-224 48 76 : : PUNCT eurjchem-224 48 77                     SPACE eurjchem-224 48 78 40 40 NUM eurjchem-224 48 79     SPACE eurjchem-224 48 80 ° ° NOUN eurjchem-224 48 81 c c NOUN eurjchem-224 48 82 ) ) PUNCT eurjchem-224 48 83 . . PUNCT eurjchem-224 48 84     SPACE eurjchem-224 49 1 in in ADP eurjchem-224 49 2     SPACE eurjchem-224 49 3 all all DET eurjchem-224 49 4     SPACE eurjchem-224 49 5 cases case NOUN eurjchem-224 49 6     SPACE eurjchem-224 49 7 of of ADP eurjchem-224 49 8     SPACE eurjchem-224 49 9 recrystallization recrystallization NOUN eurjchem-224 49 10     SPACE eurjchem-224 49 11 for for ADP eurjchem-224 49 12     SPACE eurjchem-224 49 13 the the DET eurjchem-224 49 14     SPACE eurjchem-224 49 15 same same ADJ eurjchem-224 49 16     SPACE eurjchem-224 49 17 physical physical ADJ eurjchem-224 49 18     SPACE eurjchem-224 49 19 mixture mixture NOUN eurjchem-224 49 20     SPACE eurjchem-224 49 21 recorded record VERB eurjchem-224 49 22     SPACE eurjchem-224 49 23 diffraction diffraction NOUN eurjchem-224 49 24     SPACE eurjchem-224 49 25 patterns pattern NOUN eurjchem-224 49 26     SPACE eurjchem-224 49 27 are be AUX eurjchem-224 49 28     SPACE eurjchem-224 49 29 identical identical ADJ eurjchem-224 49 30     SPACE eurjchem-224 49 31 i.e. i.e. X eurjchem-224 49 32     SPACE eurjchem-224 49 33 the the DET eurjchem-224 49 34     SPACE eurjchem-224 49 35 peaks peak NOUN eurjchem-224 49 36     SPACE eurjchem-224 49 37 have have VERB eurjchem-224 49 38     SPACE eurjchem-224 49 39 the the DET eurjchem-224 49 40     SPACE eurjchem-224 49 41 same same ADJ eurjchem-224 49 42     SPACE eurjchem-224 49 43 positions position NOUN eurjchem-224 49 44     SPACE eurjchem-224 49 45 and and CCONJ eurjchem-224 49 46     SPACE eurjchem-224 49 47 intensities intensity NOUN eurjchem-224 49 48 . . PUNCT eurjchem-224 49 49     SPACE eurjchem-224 50 1 thus thus ADV eurjchem-224 50 2     SPACE eurjchem-224 50 3 the the DET eurjchem-224 50 4     SPACE eurjchem-224 50 5 recrystallization recrystallization NOUN eurjchem-224 50 6     SPACE eurjchem-224 50 7 process process NOUN eurjchem-224 50 8     SPACE eurjchem-224 50 9 can can AUX eurjchem-224 50 10     SPACE eurjchem-224 50 11 be be AUX eurjchem-224 50 12     SPACE eurjchem-224 50 13 fast fast ADJ eurjchem-224 50 14     SPACE eurjchem-224 50 15 and and CCONJ eurjchem-224 50 16     SPACE eurjchem-224 50 17 using use VERB eurjchem-224 50 18     SPACE eurjchem-224 50 19 the the DET eurjchem-224 50 20     SPACE eurjchem-224 50 21 same same ADJ eurjchem-224 50 22     SPACE eurjchem-224 50 23 crystallization crystallization NOUN eurjchem-224 50 24     SPACE eurjchem-224 50 25 medium medium NOUN eurjchem-224 50 26     SPACE eurjchem-224 50 27 ( ( PUNCT eurjchem-224 50 28 meoh meoh PROPN eurjchem-224 50 29 : : PUNCT eurjchem-224 50 30 h2o h2o PROPN eurjchem-224 50 31 , , PUNCT eurjchem-224 50 32     SPACE eurjchem-224 50 33 1:1 1:1 NUM eurjchem-224 50 34 ) ) PUNCT eurjchem-224 50 35     SPACE eurjchem-224 50 36 gives give VERB eurjchem-224 50 37     SPACE eurjchem-224 50 38 repeatable repeatable ADJ eurjchem-224 50 39     SPACE eurjchem-224 50 40 results result NOUN eurjchem-224 50 41 . . PUNCT eurjchem-224 50 42         SPACE eurjchem-224 51 1 4 4 NUM eurjchem-224 51 2 . . PUNCT eurjchem-224 51 3     SPACE eurjchem-224 51 4 conclusion conclusion NOUN eurjchem-224 51 5         SPACE eurjchem-224 51 6 the the DET eurjchem-224 51 7     SPACE eurjchem-224 51 8 x‐ray x‐ray ADJ eurjchem-224 51 9     SPACE eurjchem-224 51 10 powder powder NOUN eurjchem-224 51 11     SPACE eurjchem-224 51 12 diffraction diffraction NOUN eurjchem-224 51 13     SPACE eurjchem-224 51 14 is be AUX eurjchem-224 51 15     SPACE eurjchem-224 51 16 a a DET eurjchem-224 51 17     SPACE eurjchem-224 51 18 powerful powerful ADJ eurjchem-224 51 19     SPACE eurjchem-224 51 20 and and CCONJ eurjchem-224 51 21     SPACE eurjchem-224 51 22 fast fast ADJ eurjchem-224 51 23     SPACE eurjchem-224 51 24 technique technique NOUN eurjchem-224 51 25     SPACE eurjchem-224 51 26 for for ADP eurjchem-224 51 27     SPACE eurjchem-224 51 28 the the DET eurjchem-224 51 29     SPACE eurjchem-224 51 30 identification identification NOUN eurjchem-224 51 31     SPACE eurjchem-224 51 32 of of ADP eurjchem-224 51 33     SPACE eurjchem-224 51 34 polycrystalline polycrystalline NOUN eurjchem-224 51 35     SPACE eurjchem-224 51 36 samples sample VERB eurjchem-224 51 37     SPACE eurjchem-224 52 1 [ [ X eurjchem-224 52 2 26‐ 26‐ NUM eurjchem-224 52 3 28 28 NUM eurjchem-224 52 4 ] ] PUNCT eurjchem-224 52 5 . . PUNCT eurjchem-224 52 6         SPACE eurjchem-224 52 7 however however ADV eurjchem-224 52 8 , , PUNCT eurjchem-224 52 9     SPACE eurjchem-224 52 10 quantitative quantitative ADJ eurjchem-224 52 11     SPACE eurjchem-224 52 12 analysis analysis NOUN eurjchem-224 52 13     SPACE eurjchem-224 52 14 is be AUX eurjchem-224 52 15     SPACE eurjchem-224 52 16 not not PART eurjchem-224 52 17     SPACE eurjchem-224 52 18 a a DET eurjchem-224 52 19     SPACE eurjchem-224 52 20 common common ADJ eurjchem-224 52 21     SPACE eurjchem-224 52 22 practice practice NOUN eurjchem-224 52 23 . . PUNCT eurjchem-224 52 24     SPACE eurjchem-224 53 1 it it PRON eurjchem-224 53 2     SPACE eurjchem-224 53 3 is be AUX eurjchem-224 53 4     SPACE eurjchem-224 53 5 mostly mostly ADV eurjchem-224 53 6     SPACE eurjchem-224 53 7 involved involve VERB eurjchem-224 53 8     SPACE eurjchem-224 53 9 with with ADP eurjchem-224 53 10     SPACE eurjchem-224 53 11 problems problem NOUN eurjchem-224 53 12     SPACE eurjchem-224 53 13 occurring occur VERB eurjchem-224 53 14     SPACE eurjchem-224 53 15 during during ADP eurjchem-224 53 16     SPACE eurjchem-224 53 17 determination determination NOUN eurjchem-224 53 18     SPACE eurjchem-224 53 19 of of ADP eurjchem-224 53 20     SPACE eurjchem-224 53 21 the the DET eurjchem-224 53 22     SPACE eurjchem-224 53 23 amount amount NOUN eurjchem-224 53 24     SPACE eurjchem-224 53 25 of of ADP eurjchem-224 53 26     SPACE eurjchem-224 53 27 phase phase NOUN eurjchem-224 53 28     SPACE eurjchem-224 53 29 in in ADP eurjchem-224 53 30     SPACE eurjchem-224 53 31 a a DET eurjchem-224 53 32     SPACE eurjchem-224 53 33 multiphase multiphase NOUN eurjchem-224 53 34     SPACE eurjchem-224 53 35 sample sample NOUN eurjchem-224 53 36 . . PUNCT eurjchem-224 53 37     SPACE eurjchem-224 54 1 the the DET eurjchem-224 54 2     SPACE eurjchem-224 54 3 quantity quantity NOUN eurjchem-224 54 4     SPACE eurjchem-224 54 5 of of ADP eurjchem-224 54 6     SPACE eurjchem-224 54 7 a a DET eurjchem-224 54 8     SPACE eurjchem-224 54 9 specific specific ADJ eurjchem-224 54 10     SPACE eurjchem-224 54 11 compound compound NOUN eurjchem-224 54 12     SPACE eurjchem-224 54 13 or or CCONJ eurjchem-224 54 14     SPACE eurjchem-224 54 15 compounds compound NOUN eurjchem-224 54 16     SPACE eurjchem-224 54 17 in in ADP eurjchem-224 54 18     SPACE eurjchem-224 54 19 a a DET eurjchem-224 54 20     SPACE eurjchem-224 54 21 multicomponent multicomponent NOUN eurjchem-224 54 22     SPACE eurjchem-224 54 23 sample sample NOUN eurjchem-224 54 24     SPACE eurjchem-224 54 25 can can AUX eurjchem-224 54 26     SPACE eurjchem-224 54 27 be be AUX eurjchem-224 54 28     SPACE eurjchem-224 54 29 determined determine VERB eurjchem-224 54 30     SPACE eurjchem-224 54 31 from from ADP eurjchem-224 54 32     SPACE eurjchem-224 54 33 the the DET eurjchem-224 54 34     SPACE eurjchem-224 54 35 intensities intensity NOUN eurjchem-224 54 36     SPACE eurjchem-224 54 37 of of ADP eurjchem-224 54 38     SPACE eurjchem-224 54 39 the the DET eurjchem-224 54 40     SPACE eurjchem-224 54 41 peaks peak NOUN eurjchem-224 54 42     SPACE eurjchem-224 54 43 in in ADP eurjchem-224 54 44     SPACE eurjchem-224 54 45 a a DET eurjchem-224 54 46     SPACE eurjchem-224 54 47 powder powder NOUN eurjchem-224 54 48     SPACE eurjchem-224 54 49 diffraction diffraction NOUN eurjchem-224 54 50     SPACE eurjchem-224 54 51 pattern pattern NOUN eurjchem-224 54 52     SPACE eurjchem-224 55 1 [ [ X eurjchem-224 55 2 13 13 NUM eurjchem-224 55 3 ] ] PUNCT eurjchem-224 55 4 . . PUNCT eurjchem-224 55 5     SPACE eurjchem-224 55 6 the the DET eurjchem-224 55 7     SPACE eurjchem-224 55 8 main main ADJ eurjchem-224 55 9     SPACE eurjchem-224 55 10 problem problem NOUN eurjchem-224 55 11     SPACE eurjchem-224 55 12 is be AUX eurjchem-224 55 13     SPACE eurjchem-224 55 14 the the DET eurjchem-224 55 15     SPACE eurjchem-224 55 16 accurate accurate ADJ eurjchem-224 55 17     SPACE eurjchem-224 55 18 determination determination NOUN eurjchem-224 55 19     SPACE eurjchem-224 55 20 of of ADP eurjchem-224 55 21     SPACE eurjchem-224 55 22 peak peak NOUN eurjchem-224 55 23     SPACE eurjchem-224 55 24 intensities intensity NOUN eurjchem-224 55 25 . . PUNCT eurjchem-224 55 26     SPACE eurjchem-224 56 1 the the DET eurjchem-224 56 2     SPACE eurjchem-224 56 3 absolute absolute ADJ eurjchem-224 56 4     SPACE eurjchem-224 56 5 intensity intensity NOUN eurjchem-224 56 6     SPACE eurjchem-224 56 7 measurement measurement NOUN eurjchem-224 56 8     SPACE eurjchem-224 56 9 practically practically ADV eurjchem-224 56 10     SPACE eurjchem-224 56 11 almost almost ADV eurjchem-224 56 12     SPACE eurjchem-224 56 13 can can AUX eurjchem-224 56 14 not not PART eurjchem-224 56 15     SPACE eurjchem-224 56 16 be be AUX eurjchem-224 56 17     SPACE eurjchem-224 56 18 made make VERB eurjchem-224 56 19 , , PUNCT eurjchem-224 56 20     SPACE eurjchem-224 56 21 but but CCONJ eurjchem-224 56 22     SPACE eurjchem-224 56 23 measurement measurement NOUN eurjchem-224 56 24     SPACE eurjchem-224 56 25 of of ADP eurjchem-224 56 26     SPACE eurjchem-224 56 27 relative relative ADJ eurjchem-224 56 28     SPACE eurjchem-224 56 29 intensity intensity NOUN eurjchem-224 56 30     SPACE eurjchem-224 56 31 is be AUX eurjchem-224 56 32     SPACE eurjchem-224 56 33 sufficient sufficient ADJ eurjchem-224 56 34     SPACE eurjchem-224 56 35 if if SCONJ eurjchem-224 56 36     SPACE eurjchem-224 56 37 the the DET eurjchem-224 56 38     SPACE eurjchem-224 56 39 comparative comparative ADJ eurjchem-224 56 40     SPACE eurjchem-224 56 41 analytical analytical ADJ eurjchem-224 56 42     SPACE eurjchem-224 56 43 method method NOUN eurjchem-224 56 44     SPACE eurjchem-224 56 45 is be AUX eurjchem-224 56 46     SPACE eurjchem-224 56 47 used use VERB eurjchem-224 56 48     SPACE eurjchem-224 56 49 [ [ X eurjchem-224 56 50 29 29 NUM eurjchem-224 56 51 ] ] PUNCT eurjchem-224 56 52 . . PUNCT eurjchem-224 56 53     SPACE eurjchem-224 56 54 thus thus ADV eurjchem-224 56 55     SPACE eurjchem-224 56 56 one one NUM eurjchem-224 56 57     SPACE eurjchem-224 56 58 of of ADP eurjchem-224 56 59     SPACE eurjchem-224 56 60 two two NUM eurjchem-224 56 61     SPACE eurjchem-224 56 62 methods method NOUN eurjchem-224 56 63     SPACE eurjchem-224 56 64 can can AUX eurjchem-224 56 65     SPACE eurjchem-224 56 66 be be AUX eurjchem-224 56 67     SPACE eurjchem-224 56 68 considered consider VERB eurjchem-224 56 69 : : PUNCT eurjchem-224 56 70     SPACE eurjchem-224 56 71 the the DET eurjchem-224 56 72     SPACE eurjchem-224 56 73 calibration calibration NOUN eurjchem-224 56 74     SPACE eurjchem-224 56 75 curve curve NOUN eurjchem-224 56 76     SPACE eurjchem-224 56 77 and and CCONJ eurjchem-224 56 78     SPACE eurjchem-224 56 79 the the DET eurjchem-224 56 80     SPACE eurjchem-224 56 81 internal internal ADJ eurjchem-224 56 82     SPACE eurjchem-224 56 83 standard standard NOUN eurjchem-224 56 84     SPACE eurjchem-224 56 85 method method NOUN eurjchem-224 56 86 . . PUNCT eurjchem-224 56 87     SPACE eurjchem-224 57 1 as as SCONJ eurjchem-224 57 2     SPACE eurjchem-224 57 3 shown show VERB eurjchem-224 57 4     SPACE eurjchem-224 57 5 in in ADP eurjchem-224 57 6     SPACE eurjchem-224 57 7 the the DET eurjchem-224 57 8     SPACE eurjchem-224 57 9 amino amino NOUN eurjchem-224 57 10     SPACE eurjchem-224 57 11 acids acid NOUN eurjchem-224 57 12     SPACE eurjchem-224 57 13 samples sample NOUN eurjchem-224 57 14     SPACE eurjchem-224 57 15 considered consider VERB eurjchem-224 57 16     SPACE eurjchem-224 57 17 here here ADV eurjchem-224 57 18 , , PUNCT eurjchem-224 57 19     SPACE eurjchem-224 57 20 the the DET eurjchem-224 57 21     SPACE eurjchem-224 57 22 relative relative ADJ eurjchem-224 57 23     SPACE eurjchem-224 57 24 intensity intensity NOUN eurjchem-224 57 25     SPACE eurjchem-224 57 26 is be AUX eurjchem-224 57 27     SPACE eurjchem-224 57 28 linearly linearly ADV eurjchem-224 57 29     SPACE eurjchem-224 57 30 correlated correlated AUX eurjchem-224 57 31     SPACE eurjchem-224 57 32 with with ADP eurjchem-224 57 33     SPACE eurjchem-224 57 34 the the DET eurjchem-224 57 35     SPACE eurjchem-224 57 36 ee ee NOUN eurjchem-224 57 37 , , PUNCT eurjchem-224 57 38     SPACE eurjchem-224 57 39 and and CCONJ eurjchem-224 57 40 , , PUNCT eurjchem-224 57 41     SPACE eurjchem-224 57 42 as as SCONJ eurjchem-224 57 43     SPACE eurjchem-224 57 44 expected expect VERB eurjchem-224 57 45 , , PUNCT eurjchem-224 57 46     SPACE eurjchem-224 57 47 it it PRON eurjchem-224 57 48     SPACE eurjchem-224 57 49 changes change VERB eurjchem-224 57 50     SPACE eurjchem-224 57 51 with with ADP eurjchem-224 57 52     SPACE eurjchem-224 57 53 the the DET eurjchem-224 57 54     SPACE eurjchem-224 57 55 degree degree NOUN eurjchem-224 57 56     SPACE eurjchem-224 57 57 of of ADP eurjchem-224 57 58     SPACE eurjchem-224 57 59 crystallinity crystallinity NOUN eurjchem-224 57 60 . . PUNCT eurjchem-224 57 61     SPACE eurjchem-224 57 62 thus thus ADV eurjchem-224 57 63     SPACE eurjchem-224 57 64 choosing choose VERB eurjchem-224 57 65     SPACE eurjchem-224 57 66 the the DET eurjchem-224 57 67     SPACE eurjchem-224 57 68 calibration calibration NOUN eurjchem-224 57 69     SPACE eurjchem-224 57 70 curve curve NOUN eurjchem-224 57 71     SPACE eurjchem-224 57 72 method method NOUN eurjchem-224 57 73     SPACE eurjchem-224 57 74 after after ADP eurjchem-224 57 75     SPACE eurjchem-224 57 76 fast fast ADJ eurjchem-224 57 77     SPACE eurjchem-224 57 78 recrystallization recrystallization NOUN eurjchem-224 57 79     SPACE eurjchem-224 57 80 from from ADP eurjchem-224 57 81     SPACE eurjchem-224 57 82 the the DET eurjchem-224 57 83     SPACE eurjchem-224 57 84 same same ADJ eurjchem-224 57 85     SPACE eurjchem-224 57 86 medium medium NOUN eurjchem-224 57 87     SPACE eurjchem-224 57 88 is be AUX eurjchem-224 57 89     SPACE eurjchem-224 57 90 quicker quick ADJ eurjchem-224 57 91     SPACE eurjchem-224 57 92 and and CCONJ eurjchem-224 57 93     SPACE eurjchem-224 57 94 more more ADJ eurjchem-224 57 95     SPACE eurjchem-224 57 96 reasonable reasonable ADJ eurjchem-224 57 97     SPACE eurjchem-224 57 98 than than ADP eurjchem-224 57 99     SPACE eurjchem-224 57 100 the the DET eurjchem-224 57 101     SPACE eurjchem-224 57 102 internal internal ADJ eurjchem-224 57 103     SPACE eurjchem-224 57 104 standard standard NOUN eurjchem-224 57 105     SPACE eurjchem-224 57 106 method method NOUN eurjchem-224 57 107 , , PUNCT eurjchem-224 57 108     SPACE eurjchem-224 57 109 because because SCONJ eurjchem-224 57 110     SPACE eurjchem-224 57 111 in in ADP eurjchem-224 57 112     SPACE eurjchem-224 57 113 the the DET eurjchem-224 57 114     SPACE eurjchem-224 57 115 second second ADJ eurjchem-224 57 116     SPACE eurjchem-224 57 117 case case NOUN eurjchem-224 57 118     SPACE eurjchem-224 57 119 the the DET eurjchem-224 57 120     SPACE eurjchem-224 57 121 problem problem NOUN eurjchem-224 57 122     SPACE eurjchem-224 57 123 of of ADP eurjchem-224 57 124     SPACE eurjchem-224 57 125 the the DET eurjchem-224 57 126     SPACE eurjchem-224 57 127 crystallinity crystallinity NOUN eurjchem-224 57 128     SPACE eurjchem-224 57 129 of of ADP eurjchem-224 57 130     SPACE eurjchem-224 57 131 the the DET eurjchem-224 57 132     SPACE eurjchem-224 57 133 standard standard NOUN eurjchem-224 57 134     SPACE eurjchem-224 57 135 exists exist VERB eurjchem-224 57 136 . . PUNCT eurjchem-224 57 137     SPACE eurjchem-224 58 1 though though SCONJ eurjchem-224 58 2     SPACE eurjchem-224 58 3 this this DET eurjchem-224 58 4     SPACE eurjchem-224 58 5 problem problem NOUN eurjchem-224 58 6     SPACE eurjchem-224 58 7 can can AUX eurjchem-224 58 8     SPACE eurjchem-224 58 9 be be AUX eurjchem-224 58 10     SPACE eurjchem-224 58 11 overridden overridden ADJ eurjchem-224 58 12     SPACE eurjchem-224 58 13 by by ADP eurjchem-224 58 14     SPACE eurjchem-224 58 15 a a DET eurjchem-224 58 16     SPACE eurjchem-224 58 17 one one NUM eurjchem-224 58 18     SPACE eurjchem-224 58 19 additional additional ADJ eurjchem-224 58 20     SPACE eurjchem-224 58 21 recrystallization recrystallization NOUN eurjchem-224 58 22 , , PUNCT eurjchem-224 58 23     SPACE eurjchem-224 58 24 the the DET eurjchem-224 58 25     SPACE eurjchem-224 58 26 internal internal ADJ eurjchem-224 58 27     SPACE eurjchem-224 58 28 standard standard NOUN eurjchem-224 58 29     SPACE eurjchem-224 58 30 method method NOUN eurjchem-224 58 31     SPACE eurjchem-224 58 32 will will AUX eurjchem-224 58 33     SPACE eurjchem-224 58 34 be be AUX eurjchem-224 58 35     SPACE eurjchem-224 58 36 still still ADV eurjchem-224 58 37     SPACE eurjchem-224 58 38 more more ADV eurjchem-224 58 39     SPACE eurjchem-224 58 40 laborious laborious ADJ eurjchem-224 58 41 , , PUNCT eurjchem-224 58 42     SPACE eurjchem-224 58 43 as as SCONJ eurjchem-224 58 44     SPACE eurjchem-224 58 45 depicted depict VERB eurjchem-224 58 46     SPACE eurjchem-224 58 47 in in ADP eurjchem-224 58 48     SPACE eurjchem-224 58 49 the the DET eurjchem-224 58 50     SPACE eurjchem-224 58 51 work work NOUN eurjchem-224 58 52     SPACE eurjchem-224 58 53 of of ADP eurjchem-224 58 54     SPACE eurjchem-224 58 55 phandnis phandnis PROPN eurjchem-224 58 56     SPACE eurjchem-224 58 57 and and CCONJ eurjchem-224 58 58     SPACE eurjchem-224 58 59 suryanarayanan suryanarayanan NOUN eurjchem-224 58 60     SPACE eurjchem-224 59 1 [ [ X eurjchem-224 59 2 7 7 NUM eurjchem-224 59 3 ] ] PUNCT eurjchem-224 59 4 . . PUNCT eurjchem-224 59 5         SPACE eurjchem-224 59 6 acknowledgement acknowledgement NOUN eurjchem-224 59 7         SPACE eurjchem-224 59 8 this this DET eurjchem-224 59 9     SPACE eurjchem-224 59 10 work work NOUN eurjchem-224 59 11     SPACE eurjchem-224 59 12 was be AUX eurjchem-224 59 13     SPACE eurjchem-224 59 14 supported support VERB eurjchem-224 59 15     SPACE eurjchem-224 59 16 by by ADP eurjchem-224 59 17     SPACE eurjchem-224 59 18 funds fund NOUN eurjchem-224 59 19     SPACE eurjchem-224 59 20 allocated allocate VERB eurjchem-224 59 21     SPACE eurjchem-224 59 22 by by ADP eurjchem-224 59 23     SPACE eurjchem-224 59 24 the the DET eurjchem-224 59 25     SPACE eurjchem-224 59 26 ministry ministry NOUN eurjchem-224 59 27     SPACE eurjchem-224 59 28 of of ADP eurjchem-224 59 29     SPACE eurjchem-224 59 30 science science NOUN eurjchem-224 59 31     SPACE eurjchem-224 59 32 and and CCONJ eurjchem-224 59 33     SPACE eurjchem-224 59 34 higher high ADJ eurjchem-224 59 35     SPACE eurjchem-224 59 36 education education NOUN eurjchem-224 59 37     SPACE eurjchem-224 59 38 to to ADP eurjchem-224 59 39     SPACE eurjchem-224 59 40 the the DET eurjchem-224 59 41     SPACE eurjchem-224 59 42 institute institute NOUN eurjchem-224 59 43     SPACE eurjchem-224 59 44 of of ADP eurjchem-224 59 45     SPACE eurjchem-224 59 46 general general NOUN eurjchem-224 59 47     SPACE eurjchem-224 59 48 and and CCONJ eurjchem-224 59 49     SPACE eurjchem-224 59 50 ecological ecological ADJ eurjchem-224 59 51     SPACE eurjchem-224 59 52 chemistry chemistry NOUN eurjchem-224 59 53 , , PUNCT eurjchem-224 59 54     SPACE eurjchem-224 59 55 technical technical ADJ eurjchem-224 59 56     SPACE eurjchem-224 59 57 university university NOUN eurjchem-224 59 58     SPACE eurjchem-224 59 59 of of ADP eurjchem-224 59 60     SPACE eurjchem-224 59 61 lodz lodz NOUN eurjchem-224 59 62 . . PUNCT eurjchem-224 59 63         SPACE eurjchem-224 60 1 references reference NOUN eurjchem-224 60 2         SPACE eurjchem-224 60 3 [ [ X eurjchem-224 60 4 1 1 NUM eurjchem-224 60 5 ] ] PUNCT eurjchem-224 60 6 . . PUNCT eurjchem-224 61 1 fischer fischer PROPN eurjchem-224 61 2 , , PUNCT eurjchem-224 61 3     SPACE eurjchem-224 61 4 e. e. PROPN eurjchem-224 61 5     SPACE eurjchem-224 61 6 ber ber PROPN eurjchem-224 61 7 . . PUNCT eurjchem-224 61 8     SPACE eurjchem-224 61 9 dtsch dtsch NOUN eurjchem-224 61 10 . . PUNCT eurjchem-224 61 11     SPACE eurjchem-224 61 12 chem chem NOUN eurjchem-224 61 13 . . PUNCT eurjchem-224 61 14     SPACE eurjchem-224 62 1 ges ges PROPN eurjchem-224 62 2 . . PUNCT eurjchem-224 62 3     SPACE eurjchem-224 62 4 1904 1904 NUM eurjchem-224 62 5 , , PUNCT eurjchem-224 62 6     SPACE eurjchem-224 62 7 37 37 NUM eurjchem-224 62 8 , , PUNCT eurjchem-224 62 9     SPACE eurjchem-224 62 10 2486‐2511 2486‐2511 NUM eurjchem-224 62 11 . . PUNCT eurjchem-224 62 12       SPACE eurjchem-224 63 1 [ [ X eurjchem-224 63 2 2 2 NUM eurjchem-224 63 3 ] ] PUNCT eurjchem-224 63 4 . . PUNCT eurjchem-224 64 1 patel patel PROPN eurjchem-224 64 2 , , PUNCT eurjchem-224 64 3     SPACE eurjchem-224 64 4 m. m. NOUN eurjchem-224 64 5     SPACE eurjchem-224 64 6 s. s. PROPN eurjchem-224 64 7 ; ; PUNCT eurjchem-224 64 8     SPACE eurjchem-224 64 9 worsley worsley PROPN eurjchem-224 64 10 . . PUNCT eurjchem-224 64 11     SPACE eurjchem-224 65 1 m. m. NOUN eurjchem-224 65 2     SPACE eurjchem-224 65 3 can can AUX eurjchem-224 65 4 . . PUNCT eurjchem-224 65 5     SPACE eurjchem-224 65 6 j. j. PROPN eurjchem-224 65 7     SPACE eurjchem-224 65 8 chem chem NOUN eurjchem-224 65 9 . . PUNCT eurjchem-224 65 10     SPACE eurjchem-224 66 1 1970 1970 NUM eurjchem-224 66 2 , , PUNCT eurjchem-224 66 3     SPACE eurjchem-224 66 4 48 48 NUM eurjchem-224 66 5 , , PUNCT eurjchem-224 66 6     SPACE eurjchem-224 66 7 1881‐1884 1881‐1884 NUM eurjchem-224 66 8 . . PUNCT eurjchem-224 66 9     SPACE eurjchem-224 67 1 [ [ X eurjchem-224 67 2 3 3 NUM eurjchem-224 67 3 ] ] PUNCT eurjchem-224 67 4 . . PUNCT eurjchem-224 68 1 marvel marvel PROPN eurjchem-224 68 2 , , PUNCT eurjchem-224 68 3     SPACE eurjchem-224 68 4 c. c. PROPN eurjchem-224 68 5     SPACE eurjchem-224 68 6 s. s. PROPN eurjchem-224 68 7     SPACE eurjchem-224 68 8 org org PROPN eurjchem-224 68 9 . . PUNCT eurjchem-224 68 10     SPACE eurjchem-224 68 11 synth synth NOUN eurjchem-224 68 12 . . PUNCT eurjchem-224 68 13     SPACE eurjchem-224 69 1 1940 1940 NUM eurjchem-224 69 2 , , PUNCT eurjchem-224 69 3     SPACE eurjchem-224 69 4 20 20 NUM eurjchem-224 69 5 , , PUNCT eurjchem-224 69 6     SPACE eurjchem-224 69 7 106‐108 106‐108 NUM eurjchem-224 69 8 . . PUNCT eurjchem-224 69 9     SPACE eurjchem-224 70 1 [ [ X eurjchem-224 70 2 4 4 NUM eurjchem-224 70 3 ] ] PUNCT eurjchem-224 70 4 . . PUNCT eurjchem-224 71 1 shono shono PROPN eurjchem-224 71 2 , , PUNCT eurjchem-224 71 3     SPACE eurjchem-224 71 4 t. t. NOUN eurjchem-224 71 5 ; ; PUNCT eurjchem-224 71 6     SPACE eurjchem-224 71 7 matsumura matsumura ADJ eurjchem-224 71 8 , , PUNCT eurjchem-224 71 9     SPACE eurjchem-224 71 10 y. y. NOUN eurjchem-224 71 11 ; ; PUNCT eurjchem-224 71 12     SPACE eurjchem-224 71 13 tsubata tsubata NOUN eurjchem-224 71 14 , , PUNCT eurjchem-224 71 15     SPACE eurjchem-224 71 16 k. k. PROPN eurjchem-224 71 17     SPACE eurjchem-224 71 18 tetrahedron tetrahedron NOUN eurjchem-224 71 19     SPACE eurjchem-224 71 20 lett lett NOUN eurjchem-224 71 21 . . PUNCT eurjchem-224 71 22     SPACE eurjchem-224 71 23 1981 1981 NUM eurjchem-224 71 24 , , PUNCT eurjchem-224 71 25     SPACE eurjchem-224 71 26 22 22 NUM eurjchem-224 71 27 , , PUNCT eurjchem-224 71 28     SPACE eurjchem-224 71 29 2411‐2412 2411‐2412 NUM eurjchem-224 71 30 . . PUNCT eurjchem-224 71 31     SPACE eurjchem-224 72 1 [ [ X eurjchem-224 72 2 5 5 NUM eurjchem-224 72 3 ] ] PUNCT eurjchem-224 72 4 . . PUNCT eurjchem-224 73 1 jakubke jakubke NOUN eurjchem-224 73 2 , , PUNCT eurjchem-224 73 3     SPACE eurjchem-224 73 4 h‐d h‐d NOUN eurjchem-224 73 5 . . PROPN eurjchem-224 73 6 ; ; PUNCT eurjchem-224 73 7     SPACE eurjchem-224 73 8 jeschkeit jeschkeit NOUN eurjchem-224 73 9 , , PUNCT eurjchem-224 73 10     SPACE eurjchem-224 73 11 h. h. PROPN eurjchem-224 73 12     SPACE eurjchem-224 73 13 aminosäuren aminosäuren PROPN eurjchem-224 73 14 , , PUNCT eurjchem-224 73 15     SPACE eurjchem-224 73 16 peptide peptide VERB eurjchem-224 73 17 , , PUNCT eurjchem-224 73 18     SPACE eurjchem-224 73 19 proteine proteine NOUN eurjchem-224 73 20 , , PUNCT eurjchem-224 73 21     SPACE eurjchem-224 73 22 akademie‐verlag akademie‐verlag NOUN eurjchem-224 73 23 , , PUNCT eurjchem-224 73 24     SPACE eurjchem-224 73 25 berlin berlin PROPN eurjchem-224 73 26     SPACE eurjchem-224 73 27 1982 1982 NUM eurjchem-224 73 28 . . PUNCT eurjchem-224 73 29     SPACE eurjchem-224 74 1 [ [ X eurjchem-224 74 2 6 6 NUM eurjchem-224 74 3 ] ] PUNCT eurjchem-224 74 4 . . PUNCT eurjchem-224 74 5 adams adams PROPN eurjchem-224 74 6 , , PUNCT eurjchem-224 74 7     SPACE eurjchem-224 74 8 s. s. PROPN eurjchem-224 74 9     SPACE eurjchem-224 74 10 s. s. PROPN eurjchem-224 74 11 ; ; PUNCT eurjchem-224 74 12     SPACE eurjchem-224 74 13 mccullough mccullough PROPN eurjchem-224 74 14 , , PUNCT eurjchem-224 74 15     SPACE eurjchem-224 74 16 k. k. PROPN eurjchem-224 74 17     SPACE eurjchem-224 74 18 f. f. PROPN eurjchem-224 74 19 ; ; PUNCT eurjchem-224 74 20     SPACE eurjchem-224 74 21 nicholson nicholson PROPN eurjchem-224 74 22 , , PUNCT eurjchem-224 74 23     SPACE eurjchem-224 74 24 j. j. PROPN eurjchem-224 74 25     SPACE eurjchem-224 74 26 s. s. PROPN eurjchem-224 74 27     SPACE eurjchem-224 74 28 arch arch NOUN eurjchem-224 74 29 . . PUNCT eurjchem-224 74 30     SPACE eurjchem-224 75 1 int int NOUN eurjchem-224 75 2 . . PUNCT eurjchem-224 75 3     SPACE eurjchem-224 75 4 pharmacodyn pharmacodyn ADV eurjchem-224 75 5 . . PUNCT eurjchem-224 75 6     SPACE eurjchem-224 76 1 ther ther ADV eurjchem-224 76 2 . . PUNCT eurjchem-224 76 3     SPACE eurjchem-224 77 1 1969 1969 NUM eurjchem-224 77 2 , , PUNCT eurjchem-224 77 3     SPACE eurjchem-224 77 4 178 178 NUM eurjchem-224 77 5 , , PUNCT eurjchem-224 77 6     SPACE eurjchem-224 77 7 115‐129 115‐129 PROPN eurjchem-224 77 8 . . PUNCT eurjchem-224 77 9     SPACE eurjchem-224 78 1 [ [ X eurjchem-224 78 2 7 7 NUM eurjchem-224 78 3 ] ] PUNCT eurjchem-224 78 4 . . PUNCT eurjchem-224 79 1 adams adams PROPN eurjchem-224 79 2 , , PUNCT eurjchem-224 79 3     SPACE eurjchem-224 79 4 s. s. PROPN eurjchem-224 79 5     SPACE eurjchem-224 79 6 s. s. PROPN eurjchem-224 79 7 ; ; PUNCT eurjchem-224 79 8     SPACE eurjchem-224 79 9 bough bough PROPN eurjchem-224 79 10 , , PUNCT eurjchem-224 79 11     SPACE eurjchem-224 79 12 r. r. PROPN eurjchem-224 79 13     SPACE eurjchem-224 79 14 g. g. PROPN eurjchem-224 79 15 ; ; PUNCT eurjchem-224 79 16     SPACE eurjchem-224 79 17 cliffe cliffe PROPN eurjchem-224 79 18 , , PUNCT eurjchem-224 79 19     SPACE eurjchem-224 79 20 e. e. PROPN eurjchem-224 79 21     SPACE eurjchem-224 79 22 e. e. PROPN eurjchem-224 79 23 ; ; PUNCT eurjchem-224 79 24     SPACE eurjchem-224 79 25 lessel lessel ADJ eurjchem-224 79 26 , , PUNCT eurjchem-224 79 27     SPACE eurjchem-224 79 28 b. b. PROPN eurjchem-224 79 29 ; ; PUNCT eurjchem-224 79 30     SPACE eurjchem-224 79 31 mills mill NOUN eurjchem-224 79 32 , , PUNCT eurjchem-224 79 33     SPACE eurjchem-224 79 34 r. r. PROPN eurjchem-224 79 35     SPACE eurjchem-224 79 36 f. f. PROPN eurjchem-224 79 37     SPACE eurjchem-224 79 38 toxicol toxicol PROPN eurjchem-224 79 39 . . PUNCT eurjchem-224 79 40     SPACE eurjchem-224 79 41 appl appl PROPN eurjchem-224 79 42 . . PUNCT eurjchem-224 79 43     SPACE eurjchem-224 79 44 pharmacol pharmacol PROPN eurjchem-224 79 45 . . PUNCT eurjchem-224 79 46     SPACE eurjchem-224 79 47 1969 1969 NUM eurjchem-224 79 48 , , PUNCT eurjchem-224 79 49     SPACE eurjchem-224 79 50 15 15 NUM eurjchem-224 79 51 , , PUNCT eurjchem-224 79 52     SPACE eurjchem-224 79 53 310 310 NUM eurjchem-224 79 54 330 330 NUM eurjchem-224 79 55 . . PUNCT eurjchem-224 79 56     SPACE eurjchem-224 80 1 [ [ X eurjchem-224 80 2 8 8 NUM eurjchem-224 80 3 ] ] PUNCT eurjchem-224 80 4 . . PUNCT eurjchem-224 81 1 phandnis phandnis PROPN eurjchem-224 81 2 , , PUNCT eurjchem-224 81 3     SPACE eurjchem-224 81 4 n. n. NOUN eurjchem-224 81 5     SPACE eurjchem-224 81 6 v. v. PROPN eurjchem-224 81 7 ; ; PUNCT eurjchem-224 81 8     SPACE eurjchem-224 81 9 suryanarayanan suryanarayanan NOUN eurjchem-224 81 10 , , PUNCT eurjchem-224 81 11     SPACE eurjchem-224 81 12 r. r. NOUN eurjchem-224 81 13         SPACE eurjchem-224 81 14 pharmaceutical pharmaceutical NOUN eurjchem-224 81 15     SPACE eurjchem-224 81 16 res re NOUN eurjchem-224 81 17 . . PUNCT eurjchem-224 81 18     SPACE eurjchem-224 81 19 1997 1997 NUM eurjchem-224 81 20 , , PUNCT eurjchem-224 81 21     SPACE eurjchem-224 81 22 9 9 NUM eurjchem-224 81 23 , , PUNCT eurjchem-224 81 24     SPACE eurjchem-224 81 25 1176‐1180 1176‐1180 NUM eurjchem-224 81 26 . . PUNCT eurjchem-224 81 27     SPACE eurjchem-224 82 1 [ [ X eurjchem-224 82 2 9 9 NUM eurjchem-224 82 3 ] ] PUNCT eurjchem-224 82 4 . . PUNCT eurjchem-224 83 1 sullivan sullivan PROPN eurjchem-224 83 2 , , PUNCT eurjchem-224 83 3     SPACE eurjchem-224 83 4 m. m. NOUN eurjchem-224 83 5     SPACE eurjchem-224 83 6 p. p. NOUN eurjchem-224 83 7     SPACE eurjchem-224 83 8 cancer cancer NOUN eurjchem-224 83 9     SPACE eurjchem-224 83 10 chemother chemother PROPN eurjchem-224 83 11 . . PUNCT eurjchem-224 83 12     SPACE eurjchem-224 84 1 rep rep PROPN eurjchem-224 84 2 . . PROPN eurjchem-224 84 3     SPACE eurjchem-224 84 4 1967 1967 NUM eurjchem-224 84 5 , , PUNCT eurjchem-224 84 6     SPACE eurjchem-224 84 7 51 51 NUM eurjchem-224 84 8 , , PUNCT eurjchem-224 84 9     SPACE eurjchem-224 84 10 393 393 NUM eurjchem-224 84 11 . . PUNCT eurjchem-224 84 12     SPACE eurjchem-224 85 1 [ [ X eurjchem-224 85 2 10 10 NUM eurjchem-224 85 3 ] ] PUNCT eurjchem-224 85 4 . . PUNCT eurjchem-224 86 1 hill hill PROPN eurjchem-224 86 2 , , PUNCT eurjchem-224 86 3     SPACE eurjchem-224 86 4 d. d. PROPN eurjchem-224 86 5     SPACE eurjchem-224 86 6 l. l. PROPN eurjchem-224 86 7     SPACE eurjchem-224 86 8 a a DET eurjchem-224 86 9     SPACE eurjchem-224 86 10 review review NOUN eurjchem-224 86 11     SPACE eurjchem-224 86 12 of of ADP eurjchem-224 86 13     SPACE eurjchem-224 86 14 cyclophosphamide cyclophosphamide NOUN eurjchem-224 86 15 , , PUNCT eurjchem-224 86 16     SPACE eurjchem-224 86 17 ch ch NOUN eurjchem-224 86 18 . . PUNCT eurjchem-224 86 19     SPACE eurjchem-224 86 20 c. c. PROPN eurjchem-224 86 21     SPACE eurjchem-224 86 22 thomas thomas PROPN eurjchem-224 86 23 , , PUNCT eurjchem-224 86 24     SPACE eurjchem-224 86 25 springfield springfield PROPN eurjchem-224 86 26     SPACE eurjchem-224 86 27 iii iii NOUN eurjchem-224 86 28     SPACE eurjchem-224 86 29 1975 1975 NUM eurjchem-224 86 30 . . PUNCT eurjchem-224 86 31     SPACE eurjchem-224 87 1 [ [ X eurjchem-224 87 2 11 11 NUM eurjchem-224 87 3 ] ] PUNCT eurjchem-224 87 4 . . PUNCT eurjchem-224 88 1 brock brock PROPN eurjchem-224 88 2 , , PUNCT eurjchem-224 88 3     SPACE eurjchem-224 88 4 n. n. NOUN eurjchem-224 88 5     SPACE eurjchem-224 88 6 cancer cancer NOUN eurjchem-224 88 7 . . PUNCT eurjchem-224 88 8     SPACE eurjchem-224 88 9 res re NOUN eurjchem-224 88 10 . . PUNCT eurjchem-224 88 11     SPACE eurjchem-224 88 12 1989 1989 NUM eurjchem-224 88 13 , , PUNCT eurjchem-224 88 14     SPACE eurjchem-224 88 15 41 41 NUM eurjchem-224 88 16 , , PUNCT eurjchem-224 88 17     SPACE eurjchem-224 88 18 1‐7 1‐7 NOUN eurjchem-224 88 19 . . PUNCT eurjchem-224 88 20     SPACE eurjchem-224 89 1 [ [ X eurjchem-224 89 2 12 12 NUM eurjchem-224 89 3 ] ] PUNCT eurjchem-224 89 4 . . PUNCT eurjchem-224 90 1 tadeusiak tadeusiak PROPN eurjchem-224 90 2 , , PUNCT eurjchem-224 90 3     SPACE eurjchem-224 90 4 e. e. PROPN eurjchem-224 90 5     SPACE eurjchem-224 90 6 j. j. PROPN eurjchem-224 90 7 ; ; PUNCT eurjchem-224 90 8     SPACE eurjchem-224 90 9 kruszynski kruszynski NOUN eurjchem-224 90 10 , , PUNCT eurjchem-224 90 11     SPACE eurjchem-224 90 12 r. r. PROPN eurjchem-224 90 13 ; ; PUNCT eurjchem-224 90 14     SPACE eurjchem-224 90 15 misiura misiura NOUN eurjchem-224 90 16 , , PUNCT eurjchem-224 90 17     SPACE eurjchem-224 90 18 k. k. PROPN eurjchem-224 90 19     SPACE eurjchem-224 90 20 pol pol PROPN eurjchem-224 90 21 . . PUNCT eurjchem-224 90 22     SPACE eurjchem-224 90 23 j. j. PROPN eurjchem-224 90 24     SPACE eurjchem-224 90 25 chem chem NOUN eurjchem-224 90 26 . . PUNCT eurjchem-224 90 27     SPACE eurjchem-224 90 28 2004 2004 NUM eurjchem-224 90 29 , , PUNCT eurjchem-224 90 30     SPACE eurjchem-224 90 31 78 78 NUM eurjchem-224 90 32 , , PUNCT eurjchem-224 90 33     SPACE eurjchem-224 90 34 431‐ 431‐ NUM eurjchem-224 90 35 435 435 NUM eurjchem-224 90 36 . . PUNCT eurjchem-224 90 37     SPACE eurjchem-224 91 1 [ [ X eurjchem-224 91 2 13 13 NUM eurjchem-224 91 3 ] ] PUNCT eurjchem-224 91 4 . . PUNCT eurjchem-224 91 5 klug klug PROPN eurjchem-224 91 6 , , PUNCT eurjchem-224 91 7     SPACE eurjchem-224 91 8 h.p h.p PROPN eurjchem-224 91 9 . . PROPN eurjchem-224 91 10 ; ; PUNCT eurjchem-224 91 11     SPACE eurjchem-224 91 12 alexander alexander NOUN eurjchem-224 91 13 , , PUNCT eurjchem-224 91 14     SPACE eurjchem-224 91 15 l.e l.e PROPN eurjchem-224 91 16 . . PROPN eurjchem-224 91 17     SPACE eurjchem-224 91 18 x‐ray x‐ray ADJ eurjchem-224 91 19     SPACE eurjchem-224 91 20 diffraction diffraction NOUN eurjchem-224 91 21     SPACE eurjchem-224 91 22 procedures procedure NOUN eurjchem-224 91 23     SPACE eurjchem-224 91 24 for for ADP eurjchem-224 91 25     SPACE eurjchem-224 91 26 polycrystalline polycrystalline NOUN eurjchem-224 91 27     SPACE eurjchem-224 91 28 and and CCONJ eurjchem-224 91 29     SPACE eurjchem-224 91 30 amorphous amorphous ADJ eurjchem-224 91 31     SPACE eurjchem-224 91 32 materials material NOUN eurjchem-224 91 33 , , PUNCT eurjchem-224 91 34     SPACE eurjchem-224 91 35 wiley wiley NOUN eurjchem-224 91 36 , , PUNCT eurjchem-224 91 37     SPACE eurjchem-224 91 38 new new ADJ eurjchem-224 91 39     SPACE eurjchem-224 91 40 york york PROPN eurjchem-224 91 41     SPACE eurjchem-224 91 42 1974 1974 NUM eurjchem-224 91 43 . . PUNCT eurjchem-224 91 44     SPACE eurjchem-224 92 1 [ [ X eurjchem-224 92 2 14 14 NUM eurjchem-224 92 3 ] ] PUNCT eurjchem-224 92 4 . . PUNCT eurjchem-224 93 1 harding harding PROPN eurjchem-224 93 2 , , PUNCT eurjchem-224 93 3     SPACE eurjchem-224 93 4 m. m. NOUN eurjchem-224 93 5     SPACE eurjchem-224 93 6 m. m. NOUN eurjchem-224 93 7 ; ; PUNCT eurjchem-224 93 8     SPACE eurjchem-224 93 9 howieson howieson NOUN eurjchem-224 93 10 , , PUNCT eurjchem-224 93 11     SPACE eurjchem-224 93 12 r. r. PROPN eurjchem-224 93 13     SPACE eurjchem-224 93 14 m. m. NOUN eurjchem-224 93 15     SPACE eurjchem-224 93 16 acta acta PROPN eurjchem-224 93 17     SPACE eurjchem-224 93 18 cryst cryst PROPN eurjchem-224 93 19 . . PUNCT eurjchem-224 93 20     SPACE eurjchem-224 93 21 1976 1976 NUM eurjchem-224 93 22 , , PUNCT eurjchem-224 93 23     SPACE eurjchem-224 93 24 b32 b32 PROPN eurjchem-224 93 25 , , PUNCT eurjchem-224 93 26     SPACE eurjchem-224 93 27 633‐634 633‐634 NOUN eurjchem-224 93 28 . . PUNCT eurjchem-224 93 29       SPACE eurjchem-224 94 1 [ [ X eurjchem-224 94 2 15 15 NUM eurjchem-224 94 3 ] ] PUNCT eurjchem-224 94 4 . . PUNCT eurjchem-224 95 1 coll coll PROPN eurjchem-224 95 2 , , PUNCT eurjchem-224 95 3     SPACE eurjchem-224 95 4 m. m. NOUN eurjchem-224 95 5 ; ; PUNCT eurjchem-224 95 6     SPACE eurjchem-224 95 7 solans solan NOUN eurjchem-224 95 8 , , PUNCT eurjchem-224 95 9     SPACE eurjchem-224 95 10 x. x. NOUN eurjchem-224 95 11 ; ; PUNCT eurjchem-224 95 12     SPACE eurjchem-224 95 13 font‐altaba font‐altaba PROPN eurjchem-224 95 14 , , PUNCT eurjchem-224 95 15     SPACE eurjchem-224 95 16 m. m. NOUN eurjchem-224 95 17 ; ; PUNCT eurjchem-224 95 18     SPACE eurjchem-224 95 19 subirana subirana PROPN eurjchem-224 95 20 , , PUNCT eurjchem-224 95 21     SPACE eurjchem-224 95 22 j. j. PROPN eurjchem-224 95 23     SPACE eurjchem-224 95 24 a. a. NOUN eurjchem-224 95 25     SPACE eurjchem-224 95 26 acta acta PROPN eurjchem-224 95 27     SPACE eurjchem-224 95 28 cryst cryst PROPN eurjchem-224 95 29 . . PUNCT eurjchem-224 95 30     SPACE eurjchem-224 95 31 1986 1986 NUM eurjchem-224 95 32 , , PUNCT eurjchem-224 95 33     SPACE eurjchem-224 95 34 c42 c42 VERB eurjchem-224 95 35 , , PUNCT eurjchem-224 95 36     SPACE eurjchem-224 95 37 599‐601 599‐601 NUM eurjchem-224 95 38 . . PUNCT eurjchem-224 95 39     SPACE eurjchem-224 96 1 [ [ X eurjchem-224 96 2 16 16 NUM eurjchem-224 96 3 ] ] PUNCT eurjchem-224 96 4 . . PUNCT eurjchem-224 97 1 gorbitz gorbitz PROPN eurjchem-224 97 2 , , PUNCT eurjchem-224 97 3     SPACE eurjchem-224 97 4 c. c. PROPN eurjchem-224 97 5     SPACE eurjchem-224 97 6 h. h. PROPN eurjchem-224 97 7 ; ; PUNCT eurjchem-224 97 8     SPACE eurjchem-224 97 9 dalhus dalhus PROPN eurjchem-224 97 10 , , PUNCT eurjchem-224 97 11     SPACE eurjchem-224 97 12 b. b. PROPN eurjchem-224 97 13       SPACE eurjchem-224 97 14 acta acta PROPN eurjchem-224 97 15     SPACE eurjchem-224 97 16 cryst cryst PROPN eurjchem-224 97 17 . . PUNCT eurjchem-224 97 18     SPACE eurjchem-224 97 19 1996 1996 NUM eurjchem-224 97 20 , , PUNCT eurjchem-224 97 21     SPACE eurjchem-224 97 22 c52 c52 VERB eurjchem-224 97 23 , , PUNCT eurjchem-224 97 24     SPACE eurjchem-224 97 25 1754‐1756 1754‐1756 NUM eurjchem-224 97 26 . . PUNCT eurjchem-224 97 27     SPACE eurjchem-224 98 1 [ [ X eurjchem-224 98 2 17 17 NUM eurjchem-224 98 3 ] ] PUNCT eurjchem-224 98 4 . . PUNCT eurjchem-224 99 1 torii torii PROPN eurjchem-224 99 2 , , PUNCT eurjchem-224 99 3     SPACE eurjchem-224 99 4 k. k. PROPN eurjchem-224 99 5 ; ; PUNCT eurjchem-224 99 6     SPACE eurjchem-224 99 7 iitaka iitaka ADV eurjchem-224 99 8 , , PUNCT eurjchem-224 99 9     SPACE eurjchem-224 99 10 y. y. NOUN eurjchem-224 99 11     SPACE eurjchem-224 99 12 acta acta PROPN eurjchem-224 99 13     SPACE eurjchem-224 99 14 cryst cryst PROPN eurjchem-224 99 15 . . PUNCT eurjchem-224 99 16     SPACE eurjchem-224 99 17 1970 1970 NUM eurjchem-224 99 18 , , PUNCT eurjchem-224 99 19     SPACE eurjchem-224 99 20 b26 b26 NOUN eurjchem-224 99 21 , , PUNCT eurjchem-224 99 22     SPACE eurjchem-224 99 23 1317‐1326 1317‐1326 NUM eurjchem-224 99 24 . . PUNCT eurjchem-224 99 25     SPACE eurjchem-224 100 1 [ [ X eurjchem-224 100 2 18 18 NUM eurjchem-224 100 3 ] ] PUNCT eurjchem-224 100 4 . . PUNCT eurjchem-224 101 1 dalhus dalhus PROPN eurjchem-224 101 2 , , PUNCT eurjchem-224 101 3     SPACE eurjchem-224 101 4 b. b. PROPN eurjchem-224 101 5 ; ; PUNCT eurjchem-224 101 6     SPACE eurjchem-224 101 7 gorbitz gorbitz NOUN eurjchem-224 101 8 , , PUNCT eurjchem-224 101 9     SPACE eurjchem-224 101 10 c. c. PROPN eurjchem-224 101 11     SPACE eurjchem-224 101 12 h. h. PROPN eurjchem-224 101 13     SPACE eurjchem-224 101 14 acta acta PROPN eurjchem-224 101 15     SPACE eurjchem-224 101 16 chem chem NOUN eurjchem-224 101 17 . . PUNCT eurjchem-224 101 18     SPACE eurjchem-224 101 19 scand scand PROPN eurjchem-224 101 20 . . PUNCT eurjchem-224 101 21     SPACE eurjchem-224 101 22 1996 1996 NUM eurjchem-224 101 23 , , PUNCT eurjchem-224 101 24     SPACE eurjchem-224 101 25 50 50 NUM eurjchem-224 101 26 , , PUNCT eurjchem-224 101 27     SPACE eurjchem-224 101 28 544‐548 544‐548 NUM eurjchem-224 101 29 . . PUNCT eurjchem-224 101 30     SPACE eurjchem-224 102 1 [ [ X eurjchem-224 102 2 19 19 NUM eurjchem-224 102 3 ] ] PUNCT eurjchem-224 102 4 . . PUNCT eurjchem-224 103 1 wang wang PROPN eurjchem-224 103 2 , , PUNCT eurjchem-224 103 3     SPACE eurjchem-224 103 4 w. w. PROPN eurjchem-224 103 5     SPACE eurjchem-224 103 6 q. q. PROPN eurjchem-224 103 7 ; ; PUNCT eurjchem-224 103 8     SPACE eurjchem-224 103 9 gong gong NOUN eurjchem-224 103 10 , , PUNCT eurjchem-224 103 11     SPACE eurjchem-224 103 12 y. y. PROPN eurjchem-224 103 13 ; ; PUNCT eurjchem-224 103 14     SPACE eurjchem-224 103 15 liang liang PROPN eurjchem-224 103 16 , , PUNCT eurjchem-224 103 17     SPACE eurjchem-224 103 18 z. z. PROPN eurjchem-224 103 19 ; ; PUNCT eurjchem-224 103 20     SPACE eurjchem-224 103 21 sun sun NOUN eurjchem-224 103 22 , , PUNCT eurjchem-224 103 23     SPACE eurjchem-224 103 24 f. f. PROPN eurjchem-224 103 25     SPACE eurjchem-224 103 26 l. l. PROPN eurjchem-224 103 27 ; ; PUNCT eurjchem-224 103 28     SPACE eurjchem-224 103 29 shi shi PROPN eurjchem-224 103 30 , , PUNCT eurjchem-224 103 31     SPACE eurjchem-224 103 32 d. d. PROPN eurjchem-224 103 33     SPACE eurjchem-224 103 34 x. x. PROPN eurjchem-224 103 35 ; ; PUNCT eurjchem-224 103 36     SPACE eurjchem-224 103 37 gao gao PROPN eurjchem-224 103 38 , , PUNCT eurjchem-224 103 39     SPACE eurjchem-224 103 40 h. h. PROPN eurjchem-224 103 41     SPACE eurjchem-224 103 42 j. j. PROPN eurjchem-224 103 43 ; ; PUNCT eurjchem-224 103 44     SPACE eurjchem-224 103 45 lin lin PROPN eurjchem-224 103 46     SPACE eurjchem-224 103 47 x. x. PROPN eurjchem-224 103 48 ; ; PUNCT eurjchem-224 103 49     SPACE eurjchem-224 103 50 jiang jiang PROPN eurjchem-224 103 51 , , PUNCT eurjchem-224 103 52     SPACE eurjchem-224 103 53 p p NOUN eurjchem-224 103 54 ; ; PUNCT eurjchem-224 103 55     SPACE eurjchem-224 103 56 wang wang PROPN eurjchem-224 103 57 , , PUNCT eurjchem-224 103 58     SPACE eurjchem-224 103 59 z. z. PROPN eurjchem-224 103 60     SPACE eurjchem-224 103 61 m. m. NOUN eurjchem-224 103 62       SPACE eurjchem-224 103 63 surf surf PROPN eurjchem-224 103 64 . . PUNCT eurjchem-224 103 65     SPACE eurjchem-224 103 66 sci sci PROPN eurjchem-224 103 67 . . PUNCT eurjchem-224 103 68     SPACE eurjchem-224 103 69 2002 2002 NUM eurjchem-224 103 70 , , PUNCT eurjchem-224 103 71     SPACE eurjchem-224 103 72 512 512 NUM eurjchem-224 103 73 , , PUNCT eurjchem-224 103 74     SPACE eurjchem-224 103 75 379‐384 379‐384 NUM eurjchem-224 103 76 . . PUNCT eurjchem-224 103 77     SPACE eurjchem-224 104 1 [ [ X eurjchem-224 104 2 20 20 NUM eurjchem-224 104 3 ] ] PUNCT eurjchem-224 104 4 . . PUNCT eurjchem-224 105 1 blasio blasio ADJ eurjchem-224 105 2 , , PUNCT eurjchem-224 105 3     SPACE eurjchem-224 105 4 b. b. PROPN eurjchem-224 105 5 ; ; PUNCT eurjchem-224 105 6     SPACE eurjchem-224 105 7 pedone pedone NOUN eurjchem-224 105 8 , , PUNCT eurjchem-224 105 9     SPACE eurjchem-224 105 10 c. c. NOUN eurjchem-224 105 11 ; ; PUNCT eurjchem-224 105 12     SPACE eurjchem-224 105 13 sirigu sirigu VERB eurjchem-224 105 14 , , PUNCT eurjchem-224 105 15     SPACE eurjchem-224 105 16 a. a. NOUN eurjchem-224 105 17     SPACE eurjchem-224 105 18 acta acta PROPN eurjchem-224 105 19     SPACE eurjchem-224 105 20 cryst cryst PROPN eurjchem-224 105 21 . . PUNCT eurjchem-224 105 22     SPACE eurjchem-224 106 1 1975 1975 NUM eurjchem-224 106 2 , , PUNCT eurjchem-224 106 3     SPACE eurjchem-224 106 4 b31 b31 NOUN eurjchem-224 106 5 , , PUNCT eurjchem-224 106 6     SPACE eurjchem-224 106 7 601 601 NUM eurjchem-224 106 8 ; ; PUNCT eurjchem-224 106 9     SPACE eurjchem-224 106 10 erratum erratum PROPN eurjchem-224 106 11     SPACE eurjchem-224 106 12 acta acta PROPN eurjchem-224 106 13     SPACE eurjchem-224 106 14 cryst cryst PROPN eurjchem-224 106 15 . . PUNCT eurjchem-224 106 16     SPACE eurjchem-224 107 1 1975 1975 NUM eurjchem-224 107 2 , , PUNCT eurjchem-224 107 3     SPACE eurjchem-224 107 4 b31 b31 NOUN eurjchem-224 107 5 , , PUNCT eurjchem-224 107 6     SPACE eurjchem-224 107 7 601‐602 601‐602 PROPN eurjchem-224 107 8 . . PUNCT eurjchem-224 107 9     SPACE eurjchem-224 108 1 [ [ X eurjchem-224 108 2 21 21 NUM eurjchem-224 108 3 ] ] PUNCT eurjchem-224 108 4 . . PUNCT eurjchem-224 109 1 moller moller PROPN eurjchem-224 109 2 , , PUNCT eurjchem-224 109 3     SPACE eurjchem-224 109 4 a. a. NOUN eurjchem-224 109 5     SPACE eurjchem-224 109 6 acta acta PROPN eurjchem-224 109 7     SPACE eurjchem-224 109 8 chem chem NOUN eurjchem-224 109 9 . . PUNCT eurjchem-224 109 10     SPACE eurjchem-224 109 11 scand scand PROPN eurjchem-224 109 12 . . PUNCT eurjchem-224 109 13     SPACE eurjchem-224 109 14 1949 1949 NUM eurjchem-224 109 15 , , PUNCT eurjchem-224 109 16     SPACE eurjchem-224 109 17 3 3 NUM eurjchem-224 109 18 , , PUNCT eurjchem-224 109 19     SPACE eurjchem-224 109 20 1326‐1330 1326‐1330 NUM eurjchem-224 109 21 . . PUNCT eurjchem-224 109 22     SPACE eurjchem-224 110 1 [ [ X eurjchem-224 110 2 22 22 NUM eurjchem-224 110 3 ] ] PUNCT eurjchem-224 110 4 . . PUNCT eurjchem-224 111 1 mallikarjunan mallikarjunan PROPN eurjchem-224 111 2 , , PUNCT eurjchem-224 111 3     SPACE eurjchem-224 111 4 m. m. NOUN eurjchem-224 111 5 ; ; PUNCT eurjchem-224 111 6     SPACE eurjchem-224 111 7 rao rao PROPN eurjchem-224 111 8 . . PUNCT eurjchem-224 111 9     SPACE eurjchem-224 111 10 s. s. PROPN eurjchem-224 111 11     SPACE eurjchem-224 111 12 t. t. PROPN eurjchem-224 111 13     SPACE eurjchem-224 111 14 acta acta PROPN eurjchem-224 111 15     SPACE eurjchem-224 111 16 cryst cryst PROPN eurjchem-224 111 17 . . PUNCT eurjchem-224 111 18     SPACE eurjchem-224 112 1 1969 1969 NUM eurjchem-224 112 2 , , PUNCT eurjchem-224 112 3     SPACE eurjchem-224 112 4 b25 b25 NOUN eurjchem-224 112 5 , , PUNCT eurjchem-224 112 6     SPACE eurjchem-224 112 7 296‐303 296‐303 NUM eurjchem-224 112 8 . . PUNCT eurjchem-224 112 9     SPACE eurjchem-224 113 1 [ [ X eurjchem-224 113 2 23 23 NUM eurjchem-224 113 3 ] ] PUNCT eurjchem-224 113 4 . . PUNCT eurjchem-224 114 1 dawson dawson PROPN eurjchem-224 114 2 , , PUNCT eurjchem-224 114 3     SPACE eurjchem-224 114 4 b. b. PROPN eurjchem-224 114 5 ; ; PUNCT eurjchem-224 114 6     SPACE eurjchem-224 114 7 mc mc PROPN eurjchem-224 114 8     SPACE eurjchem-224 114 9 mathieson mathieson PROPN eurjchem-224 114 10 , , PUNCT eurjchem-224 114 11     SPACE eurjchem-224 114 12 a. a. NOUN eurjchem-224 114 13     SPACE eurjchem-224 114 14 l. l. PROPN eurjchem-224 114 15     SPACE eurjchem-224 114 16 acta acta PROPN eurjchem-224 114 17     SPACE eurjchem-224 114 18 cryst cryst PROPN eurjchem-224 114 19 . . PUNCT eurjchem-224 114 20     SPACE eurjchem-224 114 21 1951 1951 NUM eurjchem-224 114 22 , , PUNCT eurjchem-224 114 23     SPACE eurjchem-224 114 24 4 4 NUM eurjchem-224 114 25 , , PUNCT eurjchem-224 114 26     SPACE eurjchem-224 114 27 475‐477 475‐477 NOUN eurjchem-224 114 28 . . PUNCT eurjchem-224 114 29     SPACE eurjchem-224 115 1 [ [ X eurjchem-224 115 2 24 24 NUM eurjchem-224 115 3 ] ] PUNCT eurjchem-224 115 4 . . PUNCT eurjchem-224 116 1 dalhus dalhus PROPN eurjchem-224 116 2 , , PUNCT eurjchem-224 116 3     SPACE eurjchem-224 116 4 b. b. PROPN eurjchem-224 116 5 ; ; PUNCT eurjchem-224 116 6     SPACE eurjchem-224 116 7 gorbitz gorbitz NOUN eurjchem-224 116 8 , , PUNCT eurjchem-224 116 9     SPACE eurjchem-224 116 10 c. c. PROPN eurjchem-224 116 11     SPACE eurjchem-224 116 12 h. h. PROPN eurjchem-224 116 13     SPACE eurjchem-224 116 14 acta acta PROPN eurjchem-224 116 15     SPACE eurjchem-224 116 16 cryst cryst PROPN eurjchem-224 116 17 . . PUNCT eurjchem-224 116 18     SPACE eurjchem-224 116 19 1996 1996 NUM eurjchem-224 116 20 , , PUNCT eurjchem-224 116 21     SPACE eurjchem-224 116 22 c52 c52 VERB eurjchem-224 116 23 , , PUNCT eurjchem-224 116 24     SPACE eurjchem-224 116 25 1759‐1761 1759‐1761 NUM eurjchem-224 116 26 . . PUNCT eurjchem-224 116 27     SPACE eurjchem-224 117 1 [ [ X eurjchem-224 117 2 25 25 NUM eurjchem-224 117 3 ] ] PUNCT eurjchem-224 117 4 . . PUNCT eurjchem-224 118 1 flaig flaig PROPN eurjchem-224 118 2 , , PUNCT eurjchem-224 118 3     SPACE eurjchem-224 118 4 r. r. PROPN eurjchem-224 118 5 ; ; PUNCT eurjchem-224 118 6     SPACE eurjchem-224 118 7 koritsanszky koritsanszky ADJ eurjchem-224 118 8 , , PUNCT eurjchem-224 118 9     SPACE eurjchem-224 118 10 t. t. NOUN eurjchem-224 118 11 ; ; PUNCT eurjchem-224 118 12     SPACE eurjchem-224 118 13 dittrich dittrich NOUN eurjchem-224 118 14 , , PUNCT eurjchem-224 118 15     SPACE eurjchem-224 118 16 b. b. PROPN eurjchem-224 118 17 ; ; PUNCT eurjchem-224 118 18     SPACE eurjchem-224 118 19 wagner wagner PROPN eurjchem-224 118 20 , , PUNCT eurjchem-224 118 21     SPACE eurjchem-224 118 22 a. a. NOUN eurjchem-224 118 23 ; ; PUNCT eurjchem-224 118 24     SPACE eurjchem-224 118 25 luger luger NOUN eurjchem-224 118 26 , , PUNCT eurjchem-224 118 27     SPACE eurjchem-224 118 28 p. p. NOUN eurjchem-224 118 29         SPACE eurjchem-224 118 30 j. j. PROPN eurjchem-224 118 31     SPACE eurjchem-224 118 32 am be AUX eurjchem-224 118 33 . . PUNCT eurjchem-224 118 34     SPACE eurjchem-224 118 35 chem chem NOUN eurjchem-224 118 36 . . PUNCT eurjchem-224 118 37     SPACE eurjchem-224 118 38 soc soc PROPN eurjchem-224 118 39 . . PUNCT eurjchem-224 118 40     SPACE eurjchem-224 119 1 2002 2002 NUM eurjchem-224 119 2 , , PUNCT eurjchem-224 119 3     SPACE eurjchem-224 119 4 124 124 NUM eurjchem-224 119 5 , , PUNCT eurjchem-224 119 6     SPACE eurjchem-224 119 7 3407‐3417 3407‐3417 NUM eurjchem-224 119 8 . . PUNCT eurjchem-224 119 9     SPACE eurjchem-224 120 1 [ [ X eurjchem-224 120 2 26 26 NUM eurjchem-224 120 3 ] ] PUNCT eurjchem-224 120 4 . . PUNCT eurjchem-224 121 1 jenkins jenkins PROPN eurjchem-224 121 2 , , PUNCT eurjchem-224 121 3     SPACE eurjchem-224 121 4 r. r. PROPN eurjchem-224 121 5 ; ; PUNCT eurjchem-224 121 6     SPACE eurjchem-224 121 7 snyder snyder NOUN eurjchem-224 121 8 , , PUNCT eurjchem-224 121 9     SPACE eurjchem-224 121 10 r. r. PROPN eurjchem-224 121 11     SPACE eurjchem-224 121 12 l. l. PROPN eurjchem-224 121 13     SPACE eurjchem-224 121 14 introduction introduction NOUN eurjchem-224 121 15     SPACE eurjchem-224 121 16 to to ADP eurjchem-224 121 17     SPACE eurjchem-224 121 18 x‐ray x‐ray VERB eurjchem-224 121 19     SPACE eurjchem-224 121 20 powder powder NOUN eurjchem-224 121 21     SPACE eurjchem-224 121 22 diffractometry diffractometry NOUN eurjchem-224 121 23 , , PUNCT eurjchem-224 121 24     SPACE eurjchem-224 121 25 john john PROPN eurjchem-224 121 26     SPACE eurjchem-224 121 27 wiley wiley PROPN eurjchem-224 121 28     SPACE eurjchem-224 121 29 & & CCONJ eurjchem-224 121 30     SPACE eurjchem-224 121 31 sons son NOUN eurjchem-224 121 32 , , PUNCT eurjchem-224 121 33     SPACE eurjchem-224 121 34 inc inc PROPN eurjchem-224 121 35 . . PROPN eurjchem-224 121 36 , , PUNCT eurjchem-224 121 37     SPACE eurjchem-224 121 38 new new PROPN eurjchem-224 121 39     SPACE eurjchem-224 121 40 york york NOUN eurjchem-224 121 41     SPACE eurjchem-224 121 42 1996 1996 NUM eurjchem-224 121 43 . . PUNCT eurjchem-224 121 44     SPACE eurjchem-224 122 1 [ [ X eurjchem-224 122 2 27 27 NUM eurjchem-224 122 3 ] ] PUNCT eurjchem-224 122 4 . . PUNCT eurjchem-224 123 1 masciochi masciochi PROPN eurjchem-224 123 2 , , PUNCT eurjchem-224 123 3     SPACE eurjchem-224 123 4 n. n. PROPN eurjchem-224 123 5     SPACE eurjchem-224 123 6 the the DET eurjchem-224 123 7     SPACE eurjchem-224 123 8 rigaku rigaku NOUN eurjchem-224 123 9     SPACE eurjchem-224 123 10 j. j. PROPN eurjchem-224 123 11     SPACE eurjchem-224 123 12 1997 1997 NUM eurjchem-224 123 13 , , PUNCT eurjchem-224 123 14     SPACE eurjchem-224 123 15 14 14 NUM eurjchem-224 123 16 , , PUNCT eurjchem-224 123 17     SPACE eurjchem-224 123 18 9‐16 9‐16 NUM eurjchem-224 123 19 . . PUNCT eurjchem-224 123 20     SPACE eurjchem-224 124 1 [ [ X eurjchem-224 124 2 28 28 NUM eurjchem-224 124 3 ] ] PUNCT eurjchem-224 124 4 . . PUNCT eurjchem-224 125 1 harris harris PROPN eurjchem-224 125 2 , , PUNCT eurjchem-224 125 3     SPACE eurjchem-224 125 4 k. k. PROPN eurjchem-224 125 5     SPACE eurjchem-224 125 6 d. d. PROPN eurjchem-224 125 7     SPACE eurjchem-224 125 8 m. m. NOUN eurjchem-224 125 9 ; ; PUNCT eurjchem-224 125 10     SPACE eurjchem-224 125 11 tremayne tremayne NOUN eurjchem-224 125 12 , , PUNCT eurjchem-224 125 13     SPACE eurjchem-224 125 14 m. m. NOUN eurjchem-224 125 15 ; ; PUNCT eurjchem-224 125 16     SPACE eurjchem-224 125 17 kariuki kariuki PROPN eurjchem-224 125 18 , , PUNCT eurjchem-224 125 19     SPACE eurjchem-224 125 20 b. b. PROPN eurjchem-224 125 21     SPACE eurjchem-224 125 22 m. m. NOUN eurjchem-224 125 23     SPACE eurjchem-224 125 24 angew angew PROPN eurjchem-224 125 25 . . PUNCT eurjchem-224 125 26     SPACE eurjchem-224 125 27 chem chem NOUN eurjchem-224 125 28 . . PUNCT eurjchem-224 125 29     SPACE eurjchem-224 125 30 int int NOUN eurjchem-224 125 31 . . PUNCT eurjchem-224 125 32     SPACE eurjchem-224 126 1 ed ed NOUN eurjchem-224 126 2 . . PUNCT eurjchem-224 126 3     SPACE eurjchem-224 126 4 2001 2001 NUM eurjchem-224 126 5 , , PUNCT eurjchem-224 126 6     SPACE eurjchem-224 126 7 40 40 NUM eurjchem-224 126 8 , , PUNCT eurjchem-224 126 9     SPACE eurjchem-224 126 10 1626‐1651 1626‐1651 NUM eurjchem-224 126 11 . . PUNCT eurjchem-224 126 12     SPACE eurjchem-224 127 1 [ [ X eurjchem-224 127 2 29 29 NUM eurjchem-224 127 3 ] ] PUNCT eurjchem-224 127 4 . . PUNCT eurjchem-224 128 1 zevin zevin PROPN eurjchem-224 128 2 , , PUNCT eurjchem-224 128 3     SPACE eurjchem-224 128 4 l. l. PROPN eurjchem-224 128 5     SPACE eurjchem-224 128 6 s. s. PROPN eurjchem-224 128 7     SPACE eurjchem-224 128 8 j. j. PROPN eurjchem-224 128 9     SPACE eurjchem-224 128 10 appl appl PROPN eurjchem-224 128 11 . . PUNCT eurjchem-224 128 12     SPACE eurjchem-224 128 13 cryst cryst ADV eurjchem-224 128 14 . . PUNCT eurjchem-224 128 15     SPACE eurjchem-224 128 16 1977 1977 NUM eurjchem-224 128 17 , , PUNCT eurjchem-224 128 18     SPACE eurjchem-224 128 19 10 10 NUM eurjchem-224 128 20 , , PUNCT eurjchem-224 128 21     SPACE eurjchem-224 128 22 147­150 147­150 NUM eurjchem-224 128 23 . . PUNCT eurjchem-224 128 24         SPACE