id	sid	tid	token	lemma	pos
eurjchem-228	1	1	untitled	untitle	VERB
eurjchem-228	1	2	european	european	PROPN
eurjchem-228	1	3	journal	journal	PROPN
eurjchem-228	1	4	of	of	ADP
eurjchem-228	1	5	chemistry	chemistry	NOUN
eurjchem-228	1	6	2	2	NUM
eurjchem-228	1	7	(	(	PUNCT
eurjchem-228	1	8	2	2	NUM
eurjchem-228	1	9	)	)	PUNCT
eurjchem-228	1	10	(	(	PUNCT
eurjchem-228	1	11	2011	2011	NUM
eurjchem-228	1	12	)	)	PUNCT
eurjchem-228	1	13	168‐172	168‐172	NUM
eurjchem-228	1	14	european	european	PROPN
eurjchem-228	1	15	journal	journal	PROPN
eurjchem-228	1	16	of	of	ADP
eurjchem-228	1	17	chemistry	chemistry	NOUN
eurjchem-228	1	18	issn	issn	PROPN
eurjchem-228	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-228	1	20	(	(	PUNCT
eurjchem-228	1	21	print	print	NOUN
eurjchem-228	1	22	)	)	PUNCT
eurjchem-228	1	23	/	/	SYM
eurjchem-228	1	24	issn	issn	PROPN
eurjchem-228	1	25	2153‐2257	2153‐2257	NUM
eurjchem-228	1	26	(	(	PUNCT
eurjchem-228	1	27	online	online	ADJ
eurjchem-228	1	28	)	)	PUNCT
eurjchem-228	1	29			NOUN
eurjchem-228	1	30	2011	2011	NUM
eurjchem-228	1	31	eurjchem	eurjchem	PROPN
eurjchem-228	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-228	1	33	/	/	SYM
eurjchem-228	1	34	eurjchem.2.2.168‐172.228	eurjchem.2.2.168‐172.228	PROPN
eurjchem-228	1	35	european	european	PROPN
eurjchem-228	1	36	journal	journal	PROPN
eurjchem-228	1	37	of	of	ADP
eurjchem-228	1	38	chemistry	chemistry	PROPN
eurjchem-228	1	39	journal	journal	PROPN
eurjchem-228	1	40	homepage	homepage	NOUN
eurjchem-228	1	41	:	:	PUNCT
eurjchem-228	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-228	1	43	green	green	ADJ
eurjchem-228	1	44	methodologies	methodology	NOUN
eurjchem-228	1	45	in	in	ADP
eurjchem-228	1	46	organic	organic	ADJ
eurjchem-228	1	47	synthesis	synthesis	NOUN
eurjchem-228	1	48	:	:	PUNCT
eurjchem-228	1	49	microwave	microwave	NOUN
eurjchem-228	1	50	assisted	assist	VERB
eurjchem-228	1	51	solvent‐	solvent‐	PROPN
eurjchem-228	1	52	and	and	CCONJ
eurjchem-228	1	53	catalyst‐free	catalyst‐free	ADJ
eurjchem-228	1	54	synthesis	synthesis	NOUN
eurjchem-228	1	55	of	of	ADP
eurjchem-228	1	56	enaminones	enaminone	NOUN
eurjchem-228	1	57	and	and	CCONJ
eurjchem-228	1	58	their	their	PRON
eurjchem-228	1	59	conversion	conversion	NOUN
eurjchem-228	1	60	into	into	ADP
eurjchem-228	1	61	1,3,5‐trisubstituted	1,3,5‐trisubstituted	NUM
eurjchem-228	1	62	benzenes	benzene	NOUN
eurjchem-228	1	63	as	as	ADV
eurjchem-228	1	64	well	well	ADV
eurjchem-228	1	65	as	as	ADP
eurjchem-228	1	66	3‐aroyl‐6‐substituted	3‐aroyl‐6‐substituted	ADJ
eurjchem-228	1	67	pyridines	pyridine	NOUN
eurjchem-228	1	68	morsy	morsy	PROPN
eurjchem-228	1	69	ahmed	ahmed	PROPN
eurjchem-228	1	70	el‐apaserya	el‐apaserya	PROPN
eurjchem-228	1	71	,	,	PUNCT
eurjchem-228	1	72	b	b	PROPN
eurjchem-228	1	73	,	,	PUNCT
eurjchem-228	1	74	saleh	saleh	PROPN
eurjchem-228	1	75	mohamed	mohamed	PROPN
eurjchem-228	1	76	al‐mousawia	al‐mousawia	PROPN
eurjchem-228	1	77	,	,	PUNCT
eurjchem-228	1	78	*	*	PUNCT
eurjchem-228	1	79	and	and	CCONJ
eurjchem-228	1	80	mohamed	mohamed	PROPN
eurjchem-228	1	81	helmy	helmy	PROPN
eurjchem-228	1	82	elnagdia	elnagdia	PROPN
eurjchem-228	1	83	a	a	DET
eurjchem-228	1	84	department	department	NOUN
eurjchem-228	1	85	of	of	ADP
eurjchem-228	1	86	chemistry	chemistry	NOUN
eurjchem-228	1	87	,	,	PUNCT
eurjchem-228	1	88	faculty	faculty	NOUN
eurjchem-228	1	89	of	of	ADP
eurjchem-228	1	90	science	science	NOUN
eurjchem-228	1	91	,	,	PUNCT
eurjchem-228	1	92	kuwait	kuwait	PROPN
eurjchem-228	1	93	university	university	PROPN
eurjchem-228	1	94	,	,	PUNCT
eurjchem-228	1	95	safat	safat	NOUN
eurjchem-228	1	96	,	,	PUNCT
eurjchem-228	1	97	13060	13060	NUM
eurjchem-228	1	98	,	,	PUNCT
eurjchem-228	1	99	kuwait	kuwait	PROPN
eurjchem-228	1	100	b	b	PROPN
eurjchem-228	1	101	dyeing	dyeing	NOUN
eurjchem-228	1	102	,	,	PUNCT
eurjchem-228	1	103	printing	printing	NOUN
eurjchem-228	1	104	and	and	CCONJ
eurjchem-228	1	105	textile	textile	NOUN
eurjchem-228	1	106	auxiliaries	auxiliary	NOUN
eurjchem-228	1	107	department	department	NOUN
eurjchem-228	1	108	,	,	PUNCT
eurjchem-228	1	109	textile	textile	NOUN
eurjchem-228	1	110	research	research	NOUN
eurjchem-228	1	111	division	division	NOUN
eurjchem-228	1	112	,	,	PUNCT
eurjchem-228	1	113	national	national	ADJ
eurjchem-228	1	114	research	research	NOUN
eurjchem-228	1	115	centre	centre	PROPN
eurjchem-228	1	116	,	,	PUNCT
eurjchem-228	1	117	dokki	dokki	PROPN
eurjchem-228	1	118	,	,	PUNCT
eurjchem-228	1	119	giza	giza	PROPN
eurjchem-228	1	120	,	,	PUNCT
eurjchem-228	1	121	12622	12622	NUM
eurjchem-228	1	122	,	,	PUNCT
eurjchem-228	1	123	egypt	egypt	PROPN
eurjchem-228	1	124	*	*	PUNCT
eurjchem-228	1	125	corresponding	correspond	VERB
eurjchem-228	1	126	author	author	NOUN
eurjchem-228	1	127	at	at	ADP
eurjchem-228	1	128	:	:	PUNCT
eurjchem-228	1	129	department	department	NOUN
eurjchem-228	1	130	of	of	ADP
eurjchem-228	1	131	chemistry	chemistry	NOUN
eurjchem-228	1	132	,	,	PUNCT
eurjchem-228	1	133	faculty	faculty	NOUN
eurjchem-228	1	134	of	of	ADP
eurjchem-228	1	135	science	science	NOUN
eurjchem-228	1	136	,	,	PUNCT
eurjchem-228	1	137	kuwait	kuwait	PROPN
eurjchem-228	1	138	university	university	PROPN
eurjchem-228	1	139	,	,	PUNCT
eurjchem-228	1	140	safat	safat	NOUN
eurjchem-228	1	141	,	,	PUNCT
eurjchem-228	1	142	13060	13060	NUM
eurjchem-228	1	143	,	,	PUNCT
eurjchem-228	1	144	kuwait	kuwait	PROPN
eurjchem-228	1	145	.	.	PUNCT
eurjchem-228	2	1	tel	tel	PROPN
eurjchem-228	2	2	.	.	PUNCT
eurjchem-228	2	3	:	:	PUNCT
eurjchem-228	3	1	+96599728120	+96599728120	NUM
eurjchem-228	3	2	;	;	PUNCT
eurjchem-228	3	3	fax	fax	NOUN
eurjchem-228	3	4	:	:	PUNCT
eurjchem-228	3	5	+96524816482	+96524816482	PROPN
eurjchem-228	3	6	.	.	PUNCT
eurjchem-228	3	7	e‐mail	e‐mail	PUNCT
eurjchem-228	4	1	address	address	NOUN
eurjchem-228	4	2	:	:	PUNCT
eurjchem-228	4	3	saleh.almousawi@yahoo.com	saleh.almousawi@yahoo.com	X
eurjchem-228	4	4	(	(	PUNCT
eurjchem-228	4	5	s.m	s.m	PROPN
eurjchem-228	4	6	.	.	PROPN
eurjchem-228	4	7	al‐mousawi	al‐mousawi	PROPN
eurjchem-228	4	8	)	)	PUNCT
eurjchem-228	4	9	.	.	PUNCT
eurjchem-228	5	1	article	article	NOUN
eurjchem-228	5	2	information	information	PROPN
eurjchem-228	5	3	abstract	abstract	ADV
eurjchem-228	5	4	received	receive	VERB
eurjchem-228	5	5	:	:	PUNCT
eurjchem-228	5	6	03	03	NUM
eurjchem-228	5	7	august	august	PROPN
eurjchem-228	5	8	2010	2010	NUM
eurjchem-228	5	9	received	receive	VERB
eurjchem-228	5	10	in	in	ADP
eurjchem-228	5	11	revised	revise	VERB
eurjchem-228	5	12	form	form	NOUN
eurjchem-228	5	13	:	:	PUNCT
eurjchem-228	5	14	24	24	NUM
eurjchem-228	5	15	september	september	PROPN
eurjchem-228	5	16	2010	2010	NUM
eurjchem-228	5	17	accepted	accept	VERB
eurjchem-228	5	18	:	:	PUNCT
eurjchem-228	5	19	16	16	NUM
eurjchem-228	5	20	november	november	PROPN
eurjchem-228	5	21	2010	2010	NUM
eurjchem-228	5	22	online	online	NOUN
eurjchem-228	5	23	:	:	PUNCT
eurjchem-228	5	24	30	30	NUM
eurjchem-228	5	25	june	june	PROPN
eurjchem-228	5	26	2011	2011	NUM
eurjchem-228	5	27	keywords	keyword	NOUN
eurjchem-228	5	28	enaminones	enaminone	NOUN
eurjchem-228	5	29	were	be	AUX
eurjchem-228	5	30	obtained	obtain	VERB
eurjchem-228	5	31	in	in	ADP
eurjchem-228	5	32	good	good	ADJ
eurjchem-228	5	33	yields	yield	NOUN
eurjchem-228	5	34	via	via	ADP
eurjchem-228	5	35	condensing	condense	VERB
eurjchem-228	5	36	methyl	methyl	NOUN
eurjchem-228	5	37	ketones	ketone	NOUN
eurjchem-228	5	38	with	with	ADP
eurjchem-228	5	39	(	(	PUNCT
eurjchem-228	5	40	n	n	CCONJ
eurjchem-228	5	41	,	,	PUNCT
eurjchem-228	5	42	n‐	n‐	NOUN
eurjchem-228	5	43	dimethylformamide	dimethylformamide	PROPN
eurjchem-228	5	44	dimethyl	dimethyl	NOUN
eurjchem-228	5	45	acetal	acetal	PROPN
eurjchem-228	5	46	)	)	PUNCT
eurjchem-228	5	47	dmf‐dma	dmf‐dma	VERB
eurjchem-228	5	48	under	under	ADP
eurjchem-228	5	49	microwave	microwave	NOUN
eurjchem-228	5	50	irradiation	irradiation	NOUN
eurjchem-228	5	51	in	in	ADP
eurjchem-228	5	52	absence	absence	NOUN
eurjchem-228	5	53	of	of	ADP
eurjchem-228	5	54	solvent	solvent	NOUN
eurjchem-228	5	55	.	.	PUNCT
eurjchem-228	6	1	these	these	DET
eurjchem-228	6	2	enaminones	enaminone	NOUN
eurjchem-228	6	3	were	be	AUX
eurjchem-228	6	4	readily	readily	ADV
eurjchem-228	6	5	converted	convert	VERB
eurjchem-228	6	6	into	into	ADP
eurjchem-228	6	7	1,3,5‐trisubstituted	1,3,5‐trisubstituted	NUM
eurjchem-228	6	8	benzenes	benzene	NOUN
eurjchem-228	6	9	.	.	PUNCT
eurjchem-228	7	1	reacting	react	VERB
eurjchem-228	7	2	enaminones	enaminone	NOUN
eurjchem-228	7	3	in	in	ADP
eurjchem-228	7	4	presence	presence	NOUN
eurjchem-228	7	5	of	of	ADP
eurjchem-228	7	6	ammonium	ammonium	NOUN
eurjchem-228	7	7	acetate	acetate	NOUN
eurjchem-228	7	8	has	have	AUX
eurjchem-228	7	9	afforded	afford	VERB
eurjchem-228	7	10	pyridine	pyridine	ADJ
eurjchem-228	7	11	derivatives	derivative	NOUN
eurjchem-228	7	12	.	.	PUNCT
eurjchem-228	8	1	enaminone	enaminone	NOUN
eurjchem-228	8	2	solvent‐free	solvent‐free	NOUN
eurjchem-228	8	3	green	green	ADJ
eurjchem-228	8	4	chemistry	chemistry	NOUN
eurjchem-228	8	5	dye	dye	NOUN
eurjchem-228	8	6	intermediates	intermediate	VERB
eurjchem-228	8	7	microwave	microwave	NOUN
eurjchem-228	8	8	irradiation	irradiation	NOUN
eurjchem-228	8	9	1,3,5‐trisubstituted	1,3,5‐trisubstituted	NUM
eurjchem-228	8	10	benzenes	benzene	NOUN
eurjchem-228	8	11	1	1	NUM
eurjchem-228	8	12	.	.	PUNCT
eurjchem-228	9	1	introduction	introduction	NOUN
eurjchem-228	9	2	enaminones	enaminone	NOUN
eurjchem-228	9	3	are	be	AUX
eurjchem-228	9	4	polydentate	polydentate	ADJ
eurjchem-228	9	5	reagents	reagent	NOUN
eurjchem-228	9	6	that	that	PRON
eurjchem-228	9	7	are	be	AUX
eurjchem-228	9	8	finding	find	VERB
eurjchem-228	9	9	plenty	plenty	NOUN
eurjchem-228	9	10	of	of	ADP
eurjchem-228	9	11	neat	neat	ADJ
eurjchem-228	9	12	utilities	utility	NOUN
eurjchem-228	9	13	in	in	ADP
eurjchem-228	9	14	synthetic	synthetic	ADJ
eurjchem-228	9	15	organic	organic	ADJ
eurjchem-228	9	16	chemistry	chemistry	NOUN
eurjchem-228	9	17	[	[	X
eurjchem-228	9	18	1‐4	1‐4	X
eurjchem-228	9	19	]	]	PUNCT
eurjchem-228	9	20	and/or	and/or	CCONJ
eurjchem-228	9	21	dye	dye	NOUN
eurjchem-228	9	22	intermediates	intermediate	NOUN
eurjchem-228	9	23	[	[	X
eurjchem-228	9	24	5‐7	5‐7	NUM
eurjchem-228	9	25	]	]	X
eurjchem-228	9	26	.	.	PUNCT
eurjchem-228	10	1	microwave	microwave	NOUN
eurjchem-228	10	2	irradiation	irradiation	NOUN
eurjchem-228	10	3	has	have	AUX
eurjchem-228	10	4	been	be	AUX
eurjchem-228	10	5	frequently	frequently	ADV
eurjchem-228	10	6	used	use	VERB
eurjchem-228	10	7	in	in	ADP
eurjchem-228	10	8	diverse	diverse	ADJ
eurjchem-228	10	9	organic	organic	ADJ
eurjchem-228	10	10	transformations	transformation	NOUN
eurjchem-228	10	11	with	with	ADP
eurjchem-228	10	12	a	a	DET
eurjchem-228	10	13	remarkable	remarkable	ADJ
eurjchem-228	10	14	reduction	reduction	NOUN
eurjchem-228	10	15	in	in	ADP
eurjchem-228	10	16	reaction	reaction	NOUN
eurjchem-228	10	17	times	time	NOUN
eurjchem-228	10	18	and	and	CCONJ
eurjchem-228	10	19	,	,	PUNCT
eurjchem-228	10	20	in	in	ADP
eurjchem-228	10	21	many	many	ADJ
eurjchem-228	10	22	cases	case	NOUN
eurjchem-228	10	23	,	,	PUNCT
eurjchem-228	10	24	improving	improve	VERB
eurjchem-228	10	25	the	the	DET
eurjchem-228	10	26	yields	yield	NOUN
eurjchem-228	10	27	and	and	CCONJ
eurjchem-228	10	28	selectivity	selectivity	NOUN
eurjchem-228	10	29	of	of	ADP
eurjchem-228	10	30	the	the	DET
eurjchem-228	10	31	processes	process	NOUN
eurjchem-228	10	32	.	.	PUNCT
eurjchem-228	11	1	we	we	PRON
eurjchem-228	11	2	have	have	AUX
eurjchem-228	11	3	already	already	ADV
eurjchem-228	11	4	previously	previously	ADV
eurjchem-228	11	5	reported	report	VERB
eurjchem-228	11	6	on	on	ADP
eurjchem-228	11	7	the	the	DET
eurjchem-228	11	8	utility	utility	NOUN
eurjchem-228	11	9	of	of	ADP
eurjchem-228	11	10	enaminones	enaminone	NOUN
eurjchem-228	11	11	as	as	ADP
eurjchem-228	11	12	precursors	precursor	NOUN
eurjchem-228	11	13	to	to	ADP
eurjchem-228	11	14	polyfunctional	polyfunctional	ADJ
eurjchem-228	11	15	aromatics	aromatic	NOUN
eurjchem-228	11	16	and	and	CCONJ
eurjchem-228	11	17	heteroaromatics	heteroaromatic	NOUN
eurjchem-228	11	18	[	[	X
eurjchem-228	11	19	8,9	8,9	NUM
eurjchem-228	11	20	]	]	PUNCT
eurjchem-228	11	21	.	.	PUNCT
eurjchem-228	12	1	enaminones	enaminone	NOUN
eurjchem-228	12	2	are	be	AUX
eurjchem-228	12	3	obtained	obtain	VERB
eurjchem-228	12	4	via	via	ADP
eurjchem-228	12	5	condensing	condense	VERB
eurjchem-228	12	6	methyl	methyl	NOUN
eurjchem-228	12	7	ketones	ketone	NOUN
eurjchem-228	12	8	with	with	ADP
eurjchem-228	12	9	dmf‐dma	dmf‐dma	NOUN
eurjchem-228	12	10	,	,	PUNCT
eurjchem-228	12	11	through	through	SCONJ
eurjchem-228	12	12	pathways	pathway	NOUN
eurjchem-228	12	13	employed	employ	VERB
eurjchem-228	12	14	benzene	benzene	NOUN
eurjchem-228	12	15	as	as	ADP
eurjchem-228	12	16	solvent	solvent	NOUN
eurjchem-228	12	17	for	for	ADP
eurjchem-228	12	18	this	this	DET
eurjchem-228	12	19	condensation	condensation	NOUN
eurjchem-228	12	20	.	.	PUNCT
eurjchem-228	13	1	however	however	ADV
eurjchem-228	13	2	several	several	ADJ
eurjchem-228	13	3	authors	author	NOUN
eurjchem-228	13	4	have	have	AUX
eurjchem-228	13	5	reported	report	VERB
eurjchem-228	13	6	that	that	SCONJ
eurjchem-228	13	7	yields	yield	NOUN
eurjchem-228	13	8	are	be	AUX
eurjchem-228	13	9	quite	quite	ADV
eurjchem-228	13	10	low	low	ADJ
eurjchem-228	13	11	according	accord	VERB
eurjchem-228	13	12	to	to	ADP
eurjchem-228	13	13	this	this	DET
eurjchem-228	13	14	protocol	protocol	NOUN
eurjchem-228	14	1	[	[	X
eurjchem-228	14	2	10	10	NUM
eurjchem-228	14	3	]	]	PUNCT
eurjchem-228	14	4	.	.	PUNCT
eurjchem-228	15	1	domestic	domestic	ADJ
eurjchem-228	15	2	microwave	microwave	NOUN
eurjchem-228	15	3	irradiation	irradiation	NOUN
eurjchem-228	15	4	has	have	AUX
eurjchem-228	15	5	already	already	ADV
eurjchem-228	15	6	been	be	AUX
eurjchem-228	15	7	described	describe	VERB
eurjchem-228	15	8	in	in	ADP
eurjchem-228	15	9	the	the	DET
eurjchem-228	15	10	preparation	preparation	NOUN
eurjchem-228	15	11	of	of	ADP
eurjchem-228	15	12	enaminones	enaminone	NOUN
eurjchem-228	15	13	by	by	ADP
eurjchem-228	15	14	braibante	braibante	PROPN
eurjchem-228	15	15	et	et	PROPN
eurjchem-228	15	16	al	al	PROPN
eurjchem-228	15	17	.	.	PUNCT
eurjchem-228	16	1	[	[	X
eurjchem-228	16	2	11,12	11,12	X
eurjchem-228	16	3	]	]	PUNCT
eurjchem-228	16	4	and	and	CCONJ
eurjchem-228	16	5	by	by	ADP
eurjchem-228	16	6	hamelin	hamelin	PROPN
eurjchem-228	16	7	et	et	PROPN
eurjchem-228	16	8	al	al	PROPN
eurjchem-228	16	9	.	.	PUNCT
eurjchem-228	17	1	[	[	X
eurjchem-228	17	2	13	13	NUM
eurjchem-228	17	3	]	]	PUNCT
eurjchem-228	17	4	,	,	PUNCT
eurjchem-228	17	5	in	in	ADP
eurjchem-228	17	6	both	both	DET
eurjchem-228	17	7	cases	case	NOUN
eurjchem-228	17	8	,	,	PUNCT
eurjchem-228	17	9	either	either	CCONJ
eurjchem-228	17	10	a	a	DET
eurjchem-228	17	11	solid	solid	ADJ
eurjchem-228	17	12	support	support	NOUN
eurjchem-228	17	13	or	or	CCONJ
eurjchem-228	17	14	an	an	DET
eurjchem-228	17	15	acid	acid	NOUN
eurjchem-228	17	16	catalyst	catalyst	NOUN
eurjchem-228	17	17	was	be	AUX
eurjchem-228	17	18	employed	employ	VERB
eurjchem-228	17	19	as	as	ADP
eurjchem-228	17	20	reaction	reaction	NOUN
eurjchem-228	17	21	promoter	promoter	NOUN
eurjchem-228	17	22	.	.	PUNCT
eurjchem-228	18	1	lee	lee	PROPN
eurjchem-228	18	2	et	et	PROPN
eurjchem-228	18	3	al	al	PROPN
eurjchem-228	18	4	.	.	PUNCT
eurjchem-228	19	1	[	[	X
eurjchem-228	19	2	14	14	NUM
eurjchem-228	19	3	]	]	PUNCT
eurjchem-228	19	4	reported	report	VERB
eurjchem-228	19	5	a	a	DET
eurjchem-228	19	6	solvent‐free	solvent‐free	NOUN
eurjchem-228	19	7	microwave	microwave	NOUN
eurjchem-228	19	8	assisted	assist	VERB
eurjchem-228	19	9	preparation	preparation	NOUN
eurjchem-228	19	10	of	of	ADP
eurjchem-228	19	11	enaminones	enaminone	NOUN
eurjchem-228	19	12	in	in	ADP
eurjchem-228	19	13	a	a	DET
eurjchem-228	19	14	microwave	microwave	NOUN
eurjchem-228	19	15	(	(	PUNCT
eurjchem-228	19	16	mw	mw	NOUN
eurjchem-228	19	17	)	)	PUNCT
eurjchem-228	19	18	reactor	reactor	NOUN
eurjchem-228	19	19	,	,	PUNCT
eurjchem-228	19	20	using	use	VERB
eurjchem-228	19	21	catalytic	catalytic	ADJ
eurjchem-228	19	22	hcl	hcl	PROPN
eurjchem-228	19	23	and	and	CCONJ
eurjchem-228	19	24	an	an	DET
eurjchem-228	19	25	excess	excess	NOUN
eurjchem-228	19	26	of	of	ADP
eurjchem-228	19	27	the	the	DET
eurjchem-228	19	28	amines	amine	NOUN
eurjchem-228	19	29	.	.	PUNCT
eurjchem-228	20	1	synthesis	synthesis	NOUN
eurjchem-228	20	2	of	of	ADP
eurjchem-228	20	3	enaminones	enaminone	NOUN
eurjchem-228	20	4	in	in	ADP
eurjchem-228	20	5	absence	absence	NOUN
eurjchem-228	20	6	of	of	ADP
eurjchem-228	20	7	solvent	solvent	NOUN
eurjchem-228	20	8	has	have	AUX
eurjchem-228	20	9	been	be	AUX
eurjchem-228	20	10	reported	report	VERB
eurjchem-228	20	11	in	in	ADP
eurjchem-228	20	12	domestic	domestic	ADJ
eurjchem-228	20	13	microwave	microwave	NOUN
eurjchem-228	20	14	oven	oven	NOUN
eurjchem-228	20	15	to	to	PART
eurjchem-228	20	16	afford	afford	VERB
eurjchem-228	20	17	better	well	ADJ
eurjchem-228	20	18	yield	yield	NOUN
eurjchem-228	20	19	,	,	PUNCT
eurjchem-228	20	20	shorter	short	ADJ
eurjchem-228	20	21	reaction	reaction	NOUN
eurjchem-228	20	22	times	time	NOUN
eurjchem-228	20	23	[	[	X
eurjchem-228	20	24	15	15	NUM
eurjchem-228	20	25	]	]	PUNCT
eurjchem-228	20	26	,	,	PUNCT
eurjchem-228	20	27	but	but	CCONJ
eurjchem-228	20	28	under	under	ADP
eurjchem-228	20	29	such	such	ADJ
eurjchem-228	20	30	conditions	condition	NOUN
eurjchem-228	20	31	productions	production	NOUN
eurjchem-228	20	32	of	of	ADP
eurjchem-228	20	33	hazardous	hazardous	ADJ
eurjchem-228	20	34	vapours	vapour	NOUN
eurjchem-228	20	35	could	could	AUX
eurjchem-228	20	36	not	not	PART
eurjchem-228	20	37	be	be	AUX
eurjchem-228	20	38	avoided	avoid	VERB
eurjchem-228	20	39	.	.	PUNCT
eurjchem-228	21	1	in	in	ADP
eurjchem-228	21	2	the	the	DET
eurjchem-228	21	3	present	present	ADJ
eurjchem-228	21	4	article	article	NOUN
eurjchem-228	21	5	,	,	PUNCT
eurjchem-228	21	6	we	we	PRON
eurjchem-228	21	7	report	report	VERB
eurjchem-228	21	8	high	high	ADJ
eurjchem-228	21	9	yield	yield	NOUN
eurjchem-228	21	10	synthesis	synthesis	NOUN
eurjchem-228	21	11	of	of	ADP
eurjchem-228	21	12	enaminones	enaminone	NOUN
eurjchem-228	21	13	2a‐c	2a‐c	NOUN
eurjchem-228	21	14	via	via	ADP
eurjchem-228	21	15	reacting	react	VERB
eurjchem-228	21	16	1a‐c	1a‐c	NOUN
eurjchem-228	21	17	with	with	ADP
eurjchem-228	21	18	dmf‐dma	dmf‐dma	NOUN
eurjchem-228	21	19	in	in	ADP
eurjchem-228	21	20	a	a	DET
eurjchem-228	21	21	direct	direct	ADJ
eurjchem-228	21	22	beam	beam	NOUN
eurjchem-228	21	23	microwave	microwave	NOUN
eurjchem-228	21	24	reactor	reactor	NOUN
eurjchem-228	21	25	and	and	CCONJ
eurjchem-228	21	26	report	report	NOUN
eurjchem-228	21	27	on	on	ADP
eurjchem-228	21	28	conversion	conversion	NOUN
eurjchem-228	21	29	of	of	ADP
eurjchem-228	21	30	the	the	DET
eurjchem-228	21	31	obtained	obtain	VERB
eurjchem-228	21	32	enaminones	enaminone	NOUN
eurjchem-228	21	33	as	as	ADP
eurjchem-228	21	34	precursors	precursor	NOUN
eurjchem-228	21	35	for	for	ADP
eurjchem-228	21	36	the	the	DET
eurjchem-228	21	37	title	title	NOUN
eurjchem-228	21	38	compounds	compound	NOUN
eurjchem-228	21	39	which	which	PRON
eurjchem-228	21	40	were	be	AUX
eurjchem-228	21	41	needed	need	VERB
eurjchem-228	21	42	in	in	ADP
eurjchem-228	21	43	connection	connection	NOUN
eurjchem-228	21	44	with	with	ADP
eurjchem-228	21	45	a	a	DET
eurjchem-228	21	46	biological	biological	ADJ
eurjchem-228	21	47	chemically	chemically	ADV
eurjchem-228	21	48	programme	programme	NOUN
eurjchem-228	21	49	in	in	ADP
eurjchem-228	21	50	our	our	PRON
eurjchem-228	21	51	laboratories	laboratory	NOUN
eurjchem-228	21	52	.	.	PUNCT
eurjchem-228	22	1	2	2	X
eurjchem-228	22	2	.	.	X
eurjchem-228	22	3	experimental	experimental	ADJ
eurjchem-228	22	4	2.1	2.1	NUM
eurjchem-228	22	5	.	.	PUNCT
eurjchem-228	23	1	instrumentation	instrumentation	NOUN
eurjchem-228	23	2	melting	melting	NOUN
eurjchem-228	23	3	points	point	NOUN
eurjchem-228	23	4	are	be	AUX
eurjchem-228	23	5	uncorrected	uncorrecte	VERB
eurjchem-228	23	6	.	.	PUNCT
eurjchem-228	24	1	all	all	DET
eurjchem-228	24	2	the	the	DET
eurjchem-228	24	3	reactions	reaction	NOUN
eurjchem-228	24	4	were	be	AUX
eurjchem-228	24	5	conducted	conduct	VERB
eurjchem-228	24	6	under	under	ADP
eurjchem-228	24	7	microwave	microwave	NOUN
eurjchem-228	24	8	irradiation	irradiation	NOUN
eurjchem-228	24	9	in	in	ADP
eurjchem-228	24	10	heavy‐walled	heavy‐walled	ADJ
eurjchem-228	24	11	pyrex	pyrex	PROPN
eurjchem-228	24	12	tubes	tube	NOUN
eurjchem-228	24	13	(	(	PUNCT
eurjchem-228	24	14	capacity	capacity	NOUN
eurjchem-228	24	15	10	10	NUM
eurjchem-228	24	16	ml	ml	NOUN
eurjchem-228	24	17	)	)	PUNCT
eurjchem-228	24	18	.	.	PUNCT
eurjchem-228	25	1	microwave	microwave	NOUN
eurjchem-228	25	2	heating	heating	NOUN
eurjchem-228	25	3	was	be	AUX
eurjchem-228	25	4	carried	carry	VERB
eurjchem-228	25	5	out	out	ADP
eurjchem-228	25	6	with	with	ADP
eurjchem-228	25	7	a	a	DET
eurjchem-228	25	8	single	single	ADJ
eurjchem-228	25	9	mode	mode	NOUN
eurjchem-228	25	10	cavity	cavity	NOUN
eurjchem-228	25	11	explorer	explorer	NOUN
eurjchem-228	25	12	microwave	microwave	PROPN
eurjchem-228	25	13	synthesizer	synthesizer	NOUN
eurjchem-228	25	14	(	(	PUNCT
eurjchem-228	25	15	cem	cem	NOUN
eurjchem-228	25	16	corporation	corporation	NOUN
eurjchem-228	25	17	,	,	PUNCT
eurjchem-228	25	18	nc	nc	PROPN
eurjchem-228	25	19	,	,	PUNCT
eurjchem-228	25	20	usa	usa	PROPN
eurjchem-228	25	21	)	)	PUNCT
eurjchem-228	25	22	,	,	PUNCT
eurjchem-228	25	23	producing	produce	VERB
eurjchem-228	25	24	continuous	continuous	ADJ
eurjchem-228	25	25	irradiation	irradiation	NOUN
eurjchem-228	25	26	and	and	CCONJ
eurjchem-228	25	27	equipped	equip	VERB
eurjchem-228	25	28	with	with	ADP
eurjchem-228	25	29	simultaneous	simultaneous	ADJ
eurjchem-228	25	30	external	external	ADJ
eurjchem-228	25	31	air‐cooling	air‐coole	VERB
eurjchem-228	25	32	system	system	NOUN
eurjchem-228	25	33	.	.	PUNCT
eurjchem-228	26	1	ir	ir	PROPN
eurjchem-228	26	2	spectra	spectra	PROPN
eurjchem-228	26	3	were	be	AUX
eurjchem-228	26	4	recorded	record	VERB
eurjchem-228	26	5	in	in	ADP
eurjchem-228	26	6	kbr	kbr	PROPN
eurjchem-228	26	7	disks	disk	NOUN
eurjchem-228	26	8	using	use	VERB
eurjchem-228	26	9	a	a	DET
eurjchem-228	26	10	perkin‐elmer	perkin‐elmer	NOUN
eurjchem-228	26	11	system	system	NOUN
eurjchem-228	26	12	2000	2000	NUM
eurjchem-228	26	13	ft‐ir	ft‐ir	NOUN
eurjchem-228	26	14	spectrophoto‐meter	spectrophoto‐meter	NOUN
eurjchem-228	26	15	.	.	PUNCT
eurjchem-228	27	1	1h	1h	NUM
eurjchem-228	27	2	nmr	nmr	NOUN
eurjchem-228	27	3	(	(	PUNCT
eurjchem-228	27	4	400	400	NUM
eurjchem-228	27	5	mhz	mhz	NOUN
eurjchem-228	27	6	)	)	PUNCT
eurjchem-228	27	7	and	and	CCONJ
eurjchem-228	27	8	13c	13c	NOUN
eurjchem-228	27	9	nmr	nmr	NOUN
eurjchem-228	27	10	(	(	PUNCT
eurjchem-228	27	11	100	100	NUM
eurjchem-228	27	12	mhz	mhz	NOUN
eurjchem-228	27	13	)	)	PUNCT
eurjchem-228	27	14	spectra	spectra	NOUN
eurjchem-228	27	15	were	be	AUX
eurjchem-228	27	16	recorded	record	VERB
eurjchem-228	27	17	on	on	ADP
eurjchem-228	27	18	a	a	DET
eurjchem-228	27	19	bruker	bruker	NOUN
eurjchem-228	27	20	dpx	dpx	PROPN
eurjchem-228	27	21	400	400	NUM
eurjchem-228	27	22	,	,	PUNCT
eurjchem-228	27	23	super‐conducting	super‐conducte	VERB
eurjchem-228	27	24	nmr	nmr	NOUN
eurjchem-228	27	25	spectrometer	spectrometer	NOUN
eurjchem-228	27	26	in	in	ADP
eurjchem-228	27	27	cdcl3	cdcl3	NOUN
eurjchem-228	27	28	or	or	CCONJ
eurjchem-228	27	29	dmso‐d6	dmso‐d6	NOUN
eurjchem-228	27	30	as	as	ADP
eurjchem-228	27	31	solvent	solvent	ADJ
eurjchem-228	27	32	and	and	CCONJ
eurjchem-228	27	33	tms	tms	PROPN
eurjchem-228	27	34	as	as	ADP
eurjchem-228	27	35	internal	internal	ADJ
eurjchem-228	27	36	standard	standard	NOUN
eurjchem-228	27	37	;	;	PUNCT
eurjchem-228	27	38	chemical	chemical	ADJ
eurjchem-228	27	39	shifts	shift	NOUN
eurjchem-228	27	40	were	be	AUX
eurjchem-228	27	41	reported	report	VERB
eurjchem-228	27	42	in	in	ADP
eurjchem-228	27	43			NUM
eurjchem-228	27	44	units	unit	NOUN
eurjchem-228	27	45	(	(	PUNCT
eurjchem-228	27	46	ppm	ppm	NOUN
eurjchem-228	27	47	)	)	PUNCT
eurjchem-228	27	48	.	.	PUNCT
eurjchem-228	28	1	x‐ray	x‐ray	ADJ
eurjchem-228	28	2	crystallography	crystallography	NOUN
eurjchem-228	28	3	was	be	AUX
eurjchem-228	28	4	carried	carry	VERB
eurjchem-228	28	5	out	out	ADP
eurjchem-228	28	6	on	on	ADP
eurjchem-228	28	7	a	a	DET
eurjchem-228	28	8	kappa	kappa	ADJ
eurjchem-228	28	9	ccd	ccd	PROPN
eurjchem-228	28	10	enraf	enraf	NOUN
eurjchem-228	28	11	nonius	nonius	ADJ
eurjchem-228	29	1	fr	fr	ADJ
eurjchem-228	29	2	590	590	NUM
eurjchem-228	29	3	diffractometer	diffractometer	NOUN
eurjchem-228	29	4	,	,	PUNCT
eurjchem-228	29	5	national	national	ADJ
eurjchem-228	29	6	research	research	NOUN
eurjchem-228	29	7	center	center	NOUN
eurjchem-228	29	8	,	,	PUNCT
eurjchem-228	29	9	dokki	dokki	PROPN
eurjchem-228	29	10	,	,	PUNCT
eurjchem-228	29	11	giza	giza	PROPN
eurjchem-228	29	12	,	,	PUNCT
eurjchem-228	29	13	egypt	egypt	PROPN
eurjchem-228	29	14	(	(	PUNCT
eurjchem-228	29	15	table	table	NOUN
eurjchem-228	29	16	1	1	NUM
eurjchem-228	29	17	)	)	PUNCT
eurjchem-228	29	18	.	.	PUNCT
eurjchem-228	30	1	mass	mass	PROPN
eurjchem-228	30	2	spectra	spectra	PROPN
eurjchem-228	30	3	were	be	AUX
eurjchem-228	30	4	measured	measure	VERB
eurjchem-228	30	5	on	on	ADP
eurjchem-228	30	6	a	a	DET
eurjchem-228	30	7	vg	vg	NOUN
eurjchem-228	30	8	autospec‐q	autospec‐q	PROPN
eurjchem-228	30	9	(	(	PUNCT
eurjchem-228	30	10	high	high	ADJ
eurjchem-228	30	11	resolution	resolution	NOUN
eurjchem-228	30	12	,	,	PUNCT
eurjchem-228	30	13	high	high	ADJ
eurjchem-228	30	14	performance	performance	NOUN
eurjchem-228	30	15	,	,	PUNCT
eurjchem-228	30	16	tri‐sector	tri‐sector	PROPN
eurjchem-228	30	17	gc	gc	PROPN
eurjchem-228	30	18	/	/	SYM
eurjchem-228	30	19	ms	ms	PROPN
eurjchem-228	30	20	/	/	SYM
eurjchem-228	30	21	ms	ms	PROPN
eurjchem-228	30	22	)	)	PUNCT
eurjchem-228	30	23	.	.	PUNCT
eurjchem-228	31	1	microanalyses	microanalysis	NOUN
eurjchem-228	31	2	were	be	AUX
eurjchem-228	31	3	performed	perform	VERB
eurjchem-228	31	4	on	on	ADP
eurjchem-228	31	5	a	a	DET
eurjchem-228	31	6	leco	leco	PROPN
eurjchem-228	31	7	chns‐932	chns‐932	VERB
eurjchem-228	31	8	elemental	elemental	ADJ
eurjchem-228	31	9	analyzer	analyzer	NOUN
eurjchem-228	31	10	.	.	PUNCT
eurjchem-228	32	1	2.2	2.2	NUM
eurjchem-228	32	2	.	.	PUNCT
eurjchem-228	32	3	synthesis	synthesis	NOUN
eurjchem-228	32	4	and	and	CCONJ
eurjchem-228	32	5	purification	purification	NOUN
eurjchem-228	32	6	of	of	ADP
eurjchem-228	32	7	compounds	compound	NOUN
eurjchem-228	32	8	(	(	PUNCT
eurjchem-228	32	9	2a‐c	2a‐c	NOUN
eurjchem-228	32	10	)	)	PUNCT
eurjchem-228	32	11	and	and	CCONJ
eurjchem-228	32	12	(	(	PUNCT
eurjchem-228	32	13	3	3	X
eurjchem-228	32	14	)	)	PUNCT
eurjchem-228	32	15	a	a	DET
eurjchem-228	32	16	mixtures	mixture	NOUN
eurjchem-228	32	17	of	of	ADP
eurjchem-228	32	18	phthalimidoacetone	phthalimidoacetone	NOUN
eurjchem-228	32	19	(	(	PUNCT
eurjchem-228	32	20	1a	1a	X
eurjchem-228	32	21	)	)	PUNCT
eurjchem-228	32	22	or	or	CCONJ
eurjchem-228	32	23	2‐acetylpyrrole	2‐acetylpyrrole	NUM
eurjchem-228	32	24	(	(	PUNCT
eurjchem-228	32	25	1b	1b	NUM
eurjchem-228	32	26	)	)	PUNCT
eurjchem-228	32	27	or	or	CCONJ
eurjchem-228	32	28	acetophenone	acetophenone	NOUN
eurjchem-228	32	29	(	(	PUNCT
eurjchem-228	32	30	1c	1c	NUM
eurjchem-228	32	31	)	)	PUNCT
eurjchem-228	32	32	(	(	PUNCT
eurjchem-228	32	33	0.01	0.01	NUM
eurjchem-228	32	34	mol	mol	NOUN
eurjchem-228	32	35	)	)	PUNCT
eurjchem-228	32	36	and	and	CCONJ
eurjchem-228	32	37	dmf‐dma	dmf‐dma	INTJ
eurjchem-228	32	38	(	(	PUNCT
eurjchem-228	32	39	1.19	1.19	NUM
eurjchem-228	32	40	g	g	NOUN
eurjchem-228	32	41	,	,	PUNCT
eurjchem-228	32	42	0.01	0.01	NUM
eurjchem-228	32	43	mol	mol	NOUN
eurjchem-228	32	44	)	)	PUNCT
eurjchem-228	32	45	were	be	AUX
eurjchem-228	32	46	irradiated	irradiate	VERB
eurjchem-228	32	47	by	by	ADP
eurjchem-228	32	48	focused	focused	ADJ
eurjchem-228	32	49	microwave	microwave	NOUN
eurjchem-228	32	50	at	at	ADP
eurjchem-228	32	51	180	180	NUM
eurjchem-228	32	52	°	°	NOUN
eurjchem-228	32	53	c	c	NOUN
eurjchem-228	32	54	for	for	ADP
eurjchem-228	32	55	20	20	NUM
eurjchem-228	32	56	min	min	NOUN
eurjchem-228	32	57	for	for	ADP
eurjchem-228	32	58	product	product	NOUN
eurjchem-228	32	59	2a	2a	NUM
eurjchem-228	32	60	,	,	PUNCT
eurjchem-228	32	61	120	120	NUM
eurjchem-228	32	62	°	°	NOUN
eurjchem-228	32	63	c	c	NOUN
eurjchem-228	32	64	for	for	ADP
eurjchem-228	32	65	10	10	NUM
eurjchem-228	32	66	min	min	NOUN
eurjchem-228	32	67	for	for	ADP
eurjchem-228	32	68	product	product	NOUN
eurjchem-228	32	69	2b	2b	NOUN
eurjchem-228	32	70	,	,	PUNCT
eurjchem-228	32	71	and	and	CCONJ
eurjchem-228	32	72	120	120	NUM
eurjchem-228	32	73	°	°	NOUN
eurjchem-228	32	74	c	c	NOUN
eurjchem-228	32	75	for	for	ADP
eurjchem-228	32	76	30	30	NUM
eurjchem-228	32	77	min	min	NOUN
eurjchem-228	32	78	for	for	ADP
eurjchem-228	32	79	product	product	NOUN
eurjchem-228	32	80	2c	2c	NOUN
eurjchem-228	32	81	.	.	PUNCT
eurjchem-228	33	1	completion	completion	NOUN
eurjchem-228	33	2	of	of	ADP
eurjchem-228	33	3	the	the	DET
eurjchem-228	33	4	reactions	reaction	NOUN
eurjchem-228	33	5	was	be	AUX
eurjchem-228	33	6	monitored	monitor	VERB
eurjchem-228	33	7	by	by	ADP
eurjchem-228	33	8	tlc	tlc	PROPN
eurjchem-228	33	9	.	.	PUNCT
eurjchem-228	34	1	the	the	DET
eurjchem-228	34	2	build‐up	build‐up	PROPN
eurjchem-228	34	3	of	of	ADP
eurjchem-228	34	4	pressure	pressure	NOUN
eurjchem-228	34	5	in	in	ADP
eurjchem-228	34	6	the	the	DET
eurjchem-228	34	7	closed	closed	ADJ
eurjchem-228	34	8	el‐apasery	el‐apasery	NOUN
eurjchem-228	34	9	et	et	PROPN
eurjchem-228	34	10	al	al	PROPN
eurjchem-228	34	11	.	.	PUNCT
eurjchem-228	34	12	/	/	SYM
eurjchem-228	34	13	european	european	PROPN
eurjchem-228	34	14	journal	journal	PROPN
eurjchem-228	34	15	of	of	ADP
eurjchem-228	34	16	chemistry	chemistry	NOUN
eurjchem-228	34	17	2	2	NUM
eurjchem-228	34	18	(	(	PUNCT
eurjchem-228	34	19	2	2	NUM
eurjchem-228	34	20	)	)	PUNCT
eurjchem-228	34	21	(	(	PUNCT
eurjchem-228	34	22	2011	2011	NUM
eurjchem-228	34	23	)	)	PUNCT
eurjchem-228	34	24	168‐172	168‐172	NUM
eurjchem-228	34	25	169	169	NUM
eurjchem-228	34	26	reaction	reaction	NOUN
eurjchem-228	34	27	vessel	vessel	NOUN
eurjchem-228	34	28	was	be	AUX
eurjchem-228	34	29	carefully	carefully	ADV
eurjchem-228	34	30	monitored	monitor	VERB
eurjchem-228	34	31	.	.	PUNCT
eurjchem-228	35	1	after	after	ADP
eurjchem-228	35	2	the	the	DET
eurjchem-228	35	3	irradiation	irradiation	NOUN
eurjchem-228	35	4	,	,	PUNCT
eurjchem-228	35	5	the	the	DET
eurjchem-228	35	6	reaction	reaction	NOUN
eurjchem-228	35	7	tube	tube	NOUN
eurjchem-228	35	8	was	be	AUX
eurjchem-228	35	9	cooled	cool	VERB
eurjchem-228	35	10	with	with	ADP
eurjchem-228	35	11	high‐pressure	high‐pressure	NOUN
eurjchem-228	35	12	air	air	NOUN
eurjchem-228	35	13	through	through	ADP
eurjchem-228	35	14	an	an	DET
eurjchem-228	35	15	inbuilt	inbuilt	ADJ
eurjchem-228	35	16	system	system	NOUN
eurjchem-228	35	17	in	in	ADP
eurjchem-228	35	18	the	the	DET
eurjchem-228	35	19	instrument	instrument	NOUN
eurjchem-228	35	20	until	until	SCONJ
eurjchem-228	35	21	the	the	DET
eurjchem-228	35	22	temperature	temperature	NOUN
eurjchem-228	35	23	had	have	AUX
eurjchem-228	35	24	fallen	fall	VERB
eurjchem-228	35	25	below	below	ADP
eurjchem-228	35	26	50	50	NUM
eurjchem-228	35	27	°	°	NOUN
eurjchem-228	35	28	c	c	NOUN
eurjchem-228	35	29	.	.	PUNCT
eurjchem-228	36	1	the	the	DET
eurjchem-228	36	2	reaction	reaction	NOUN
eurjchem-228	36	3	mixture	mixture	NOUN
eurjchem-228	36	4	left	leave	VERB
eurjchem-228	36	5	to	to	PART
eurjchem-228	36	6	cool	cool	VERB
eurjchem-228	36	7	to	to	PART
eurjchem-228	36	8	room	room	VERB
eurjchem-228	36	9	temperature	temperature	NOUN
eurjchem-228	36	10	and	and	CCONJ
eurjchem-228	36	11	then	then	ADV
eurjchem-228	36	12	treated	treat	VERB
eurjchem-228	36	13	with	with	ADP
eurjchem-228	36	14	a	a	DET
eurjchem-228	36	15	mixture	mixture	NOUN
eurjchem-228	36	16	of	of	ADP
eurjchem-228	36	17	etoh	etoh	NOUN
eurjchem-228	36	18	:	:	PUNCT
eurjchem-228	36	19	dioxane	dioxane	NOUN
eurjchem-228	36	20	(	(	PUNCT
eurjchem-228	36	21	3:1	3:1	NUM
eurjchem-228	36	22	)	)	PUNCT
eurjchem-228	36	23	.	.	PUNCT
eurjchem-228	37	1	the	the	DET
eurjchem-228	37	2	solid	solid	ADJ
eurjchem-228	37	3	product	product	NOUN
eurjchem-228	37	4	,	,	PUNCT
eurjchem-228	37	5	so	so	ADV
eurjchem-228	37	6	formed	form	VERB
eurjchem-228	37	7	,	,	PUNCT
eurjchem-228	37	8	was	be	AUX
eurjchem-228	37	9	collected	collect	VERB
eurjchem-228	37	10	by	by	ADP
eurjchem-228	37	11	filtration	filtration	NOUN
eurjchem-228	37	12	and	and	CCONJ
eurjchem-228	37	13	crystallized	crystallize	VERB
eurjchem-228	37	14	from	from	ADP
eurjchem-228	37	15	dioxane	dioxane	NOUN
eurjchem-228	37	16	to	to	PART
eurjchem-228	37	17	afford	afford	VERB
eurjchem-228	37	18	compounds	compound	NOUN
eurjchem-228	37	19	2a‐c	2a‐c	NOUN
eurjchem-228	37	20	.	.	PUNCT
eurjchem-228	38	1	the	the	DET
eurjchem-228	38	2	filtrate	filtrate	NOUN
eurjchem-228	38	3	of	of	ADP
eurjchem-228	38	4	product	product	NOUN
eurjchem-228	38	5	2a	2a	NUM
eurjchem-228	38	6	was	be	AUX
eurjchem-228	38	7	dried	dry	VERB
eurjchem-228	38	8	over	over	ADP
eurjchem-228	38	9	anhydrous	anhydrous	ADJ
eurjchem-228	38	10	sodium	sodium	NOUN
eurjchem-228	38	11	sulphate	sulphate	NOUN
eurjchem-228	38	12	and	and	CCONJ
eurjchem-228	38	13	concentrated	concentrate	VERB
eurjchem-228	38	14	on	on	ADP
eurjchem-228	38	15	vacuum	vacuum	NOUN
eurjchem-228	38	16	.	.	PUNCT
eurjchem-228	39	1	the	the	DET
eurjchem-228	39	2	residue	residue	NOUN
eurjchem-228	39	3	was	be	AUX
eurjchem-228	39	4	purified	purify	VERB
eurjchem-228	39	5	by	by	ADP
eurjchem-228	39	6	column	column	NOUN
eurjchem-228	39	7	chromatography	chromatography	NOUN
eurjchem-228	39	8	on	on	ADP
eurjchem-228	39	9	silica	silica	NOUN
eurjchem-228	39	10	gel	gel	NOUN
eurjchem-228	39	11	with	with	ADP
eurjchem-228	39	12	ethyl	ethyl	PROPN
eurjchem-228	39	13	acetate	acetate	NOUN
eurjchem-228	39	14	:	:	PUNCT
eurjchem-228	39	15	etoh	etoh	NOUN
eurjchem-228	39	16	(	(	PUNCT
eurjchem-228	39	17	9:1	9:1	NUM
eurjchem-228	39	18	)	)	PUNCT
eurjchem-228	39	19	as	as	ADV
eurjchem-228	39	20	then	then	ADV
eurjchem-228	39	21	eluent	eluent	VERB
eurjchem-228	39	22	to	to	PART
eurjchem-228	39	23	afford	afford	VERB
eurjchem-228	39	24	product	product	NOUN
eurjchem-228	39	25	3	3	NUM
eurjchem-228	39	26	in	in	ADP
eurjchem-228	39	27	10	10	NUM
eurjchem-228	39	28	%	%	NOUN
eurjchem-228	39	29	yields	yield	NOUN
eurjchem-228	39	30	.	.	PUNCT
eurjchem-228	40	1	2‐(4‐dimethylamino‐2‐oxo‐but‐3‐enyl)isoindole‐1,3‐dione	2‐(4‐dimethylamino‐2‐oxo‐but‐3‐enyl)isoindole‐1,3‐dione	NUM
eurjchem-228	40	2	,	,	PUNCT
eurjchem-228	40	3	2a	2a	NUM
eurjchem-228	40	4	:	:	PUNCT
eurjchem-228	40	5	yellow	yellow	ADJ
eurjchem-228	40	6	crystals	crystal	NOUN
eurjchem-228	40	7	.	.	PUNCT
eurjchem-228	41	1	yield	yield	NOUN
eurjchem-228	41	2	:	:	PUNCT
eurjchem-228	41	3	77	77	NUM
eurjchem-228	41	4	%	%	NOUN
eurjchem-228	41	5	.	.	PUNCT
eurjchem-228	42	1	m.p	m.p	PROPN
eurjchem-228	42	2	.	.	PROPN
eurjchem-228	42	3	:	:	PUNCT
eurjchem-228	43	1	162	162	NUM
eurjchem-228	43	2	°	°	NUM
eurjchem-228	43	3	c	c	X
eurjchem-228	43	4	(	(	PUNCT
eurjchem-228	43	5	lit	lit	ADJ
eurjchem-228	43	6	.	.	PUNCT
eurjchem-228	44	1	159‐162	159‐162	NUM
eurjchem-228	45	1	°	°	PRON
eurjchem-228	45	2	c	c	NOUN
eurjchem-228	45	3	[	[	X
eurjchem-228	45	4	16	16	NUM
eurjchem-228	45	5	]	]	SYM
eurjchem-228	45	6	)	)	PUNCT
eurjchem-228	45	7	.	.	PUNCT
eurjchem-228	46	1	ft‐ir	ft‐ir	NOUN
eurjchem-228	46	2	(	(	PUNCT
eurjchem-228	46	3	kbr	kbr	PROPN
eurjchem-228	46	4	,	,	PUNCT
eurjchem-228	46	5	cm‐1	cm‐1	PROPN
eurjchem-228	46	6	):	):	PUNCT
eurjchem-228	46	7	1769	1769	NUM
eurjchem-228	46	8	,	,	PUNCT
eurjchem-228	46	9	1714	1714	NUM
eurjchem-228	46	10	,	,	PUNCT
eurjchem-228	46	11	1660	1660	NUM
eurjchem-228	46	12	(	(	PUNCT
eurjchem-228	46	13	co	co	NOUN
eurjchem-228	46	14	)	)	PUNCT
eurjchem-228	46	15	.	.	PUNCT
eurjchem-228	47	1	1h	1h	NUM
eurjchem-228	47	2	nmr	nmr	NOUN
eurjchem-228	47	3	(	(	PUNCT
eurjchem-228	47	4	400	400	NUM
eurjchem-228	47	5	mhz	mhz	NOUN
eurjchem-228	47	6	,	,	PUNCT
eurjchem-228	47	7	dmso‐d6	dmso‐d6	NUM
eurjchem-228	47	8	):	):	PUNCT
eurjchem-228	47	9	2.72	2.72	NUM
eurjchem-228	47	10	(	(	PUNCT
eurjchem-228	47	11	s	s	PROPN
eurjchem-228	47	12	,	,	PUNCT
eurjchem-228	47	13	3h	3h	NUM
eurjchem-228	47	14	,	,	PUNCT
eurjchem-228	47	15	ch3	ch3	PROPN
eurjchem-228	47	16	)	)	PUNCT
eurjchem-228	47	17	,	,	PUNCT
eurjchem-228	47	18	3.05	3.05	NUM
eurjchem-228	47	19	(	(	PUNCT
eurjchem-228	47	20	s	s	PROPN
eurjchem-228	47	21	,	,	PUNCT
eurjchem-228	47	22	3h	3h	NUM
eurjchem-228	47	23	,	,	PUNCT
eurjchem-228	47	24	ch3	ch3	PROPN
eurjchem-228	47	25	)	)	PUNCT
eurjchem-228	47	26	,	,	PUNCT
eurjchem-228	47	27	4.40	4.40	NUM
eurjchem-228	47	28	(	(	PUNCT
eurjchem-228	47	29	s	s	PROPN
eurjchem-228	47	30	,	,	PUNCT
eurjchem-228	47	31	2h	2h	NUM
eurjchem-228	47	32	,	,	PUNCT
eurjchem-228	47	33	ch2	ch2	PROPN
eurjchem-228	47	34	)	)	PUNCT
eurjchem-228	47	35	,	,	PUNCT
eurjchem-228	47	36	5.04	5.04	NUM
eurjchem-228	47	37	(	(	PUNCT
eurjchem-228	47	38	d	d	PROPN
eurjchem-228	47	39	,	,	PUNCT
eurjchem-228	47	40	1h	1h	NUM
eurjchem-228	47	41	,	,	PUNCT
eurjchem-228	47	42	j=12	j=12	PROPN
eurjchem-228	47	43	hz	hz	PROPN
eurjchem-228	47	44	,	,	PUNCT
eurjchem-228	47	45	ch	ch	NOUN
eurjchem-228	47	46	)	)	PUNCT
eurjchem-228	47	47	,	,	PUNCT
eurjchem-228	47	48	7.61	7.61	NUM
eurjchem-228	47	49	(	(	PUNCT
eurjchem-228	47	50	d	d	PROPN
eurjchem-228	47	51	,	,	PUNCT
eurjchem-228	47	52	1h	1h	NUM
eurjchem-228	47	53	,	,	PUNCT
eurjchem-228	47	54	j=12	j=12	PROPN
eurjchem-228	47	55	hz	hz	PROPN
eurjchem-228	47	56	,	,	PUNCT
eurjchem-228	47	57	ch	ch	NOUN
eurjchem-228	47	58	)	)	PUNCT
eurjchem-228	47	59	,	,	PUNCT
eurjchem-228	47	60	7.85‐	7.85‐	NUM
eurjchem-228	47	61	7.91	7.91	NUM
eurjchem-228	47	62	(	(	PUNCT
eurjchem-228	47	63	m	m	PROPN
eurjchem-228	47	64	,	,	PUNCT
eurjchem-228	47	65	4h	4h	NUM
eurjchem-228	47	66	,	,	PUNCT
eurjchem-228	47	67	phthalimidyl‐h	phthalimidyl‐h	PROPN
eurjchem-228	47	68	)	)	PUNCT
eurjchem-228	47	69	.	.	PUNCT
eurjchem-228	48	1	ms	ms	NOUN
eurjchem-228	48	2	(	(	PUNCT
eurjchem-228	48	3	ei	ei	PROPN
eurjchem-228	48	4	,	,	PUNCT
eurjchem-228	48	5	m	m	PROPN
eurjchem-228	48	6	/	/	SYM
eurjchem-228	48	7	z	z	NOUN
eurjchem-228	48	8	,	,	PUNCT
eurjchem-228	48	9	%	%	INTJ
eurjchem-228	48	10	):	):	PUNCT
eurjchem-228	48	11	258	258	NUM
eurjchem-228	49	1	[	[	X
eurjchem-228	49	2	m+	m+	NUM
eurjchem-228	49	3	,	,	PUNCT
eurjchem-228	49	4	24	24	NUM
eurjchem-228	49	5	%	%	NOUN
eurjchem-228	49	6	]	]	PUNCT
eurjchem-228	49	7	.	.	PUNCT
eurjchem-228	50	1	anal	anal	PROPN
eurjchem-228	50	2	.	.	PUNCT
eurjchem-228	50	3	calcd	calcd	NOUN
eurjchem-228	50	4	.	.	PUNCT
eurjchem-228	51	1	for	for	ADP
eurjchem-228	51	2	c14h14n2o3	c14h14n2o3	NOUN
eurjchem-228	51	3	:	:	PUNCT
eurjchem-228	51	4	c	c	X
eurjchem-228	51	5	,	,	PUNCT
eurjchem-228	51	6	65.11	65.11	NUM
eurjchem-228	51	7	;	;	PUNCT
eurjchem-228	51	8	h	h	X
eurjchem-228	51	9	,	,	PUNCT
eurjchem-228	51	10	5.46	5.46	NUM
eurjchem-228	51	11	;	;	PUNCT
eurjchem-228	51	12	n	n	CCONJ
eurjchem-228	51	13	,	,	PUNCT
eurjchem-228	51	14	10.85	10.85	NUM
eurjchem-228	51	15	.	.	PUNCT
eurjchem-228	51	16	found	find	VERB
eurjchem-228	51	17	:	:	PUNCT
eurjchem-228	52	1	c	c	X
eurjchem-228	52	2	,	,	PUNCT
eurjchem-228	52	3	65.18	65.18	NUM
eurjchem-228	52	4	;	;	PUNCT
eurjchem-228	52	5	h	h	X
eurjchem-228	52	6	,	,	PUNCT
eurjchem-228	52	7	5.44	5.44	NUM
eurjchem-228	52	8	;	;	PUNCT
eurjchem-228	52	9	n	n	CCONJ
eurjchem-228	52	10	,	,	PUNCT
eurjchem-228	52	11	10.76	10.76	NUM
eurjchem-228	52	12	.	.	PUNCT
eurjchem-228	53	1	3‐dimethylamino‐1‐(1h‐pyrrol‐2‐yl)‐propenone	3‐dimethylamino‐1‐(1h‐pyrrol‐2‐yl)‐propenone	NUM
eurjchem-228	53	2	,	,	PUNCT
eurjchem-228	53	3	2b	2b	NUM
eurjchem-228	53	4	:	:	PUNCT
eurjchem-228	53	5	orange	orange	ADJ
eurjchem-228	53	6	crystals	crystal	NOUN
eurjchem-228	53	7	.	.	PUNCT
eurjchem-228	54	1	yield	yield	NOUN
eurjchem-228	54	2	:	:	PUNCT
eurjchem-228	54	3	86	86	NUM
eurjchem-228	54	4	%	%	NOUN
eurjchem-228	54	5	.	.	PUNCT
eurjchem-228	55	1	m.p	m.p	PROPN
eurjchem-228	55	2	.	.	PROPN
eurjchem-228	55	3	:	:	PUNCT
eurjchem-228	56	1	199‐200	199‐200	NUM
eurjchem-228	56	2	°	°	PRON
eurjchem-228	56	3	c	c	X
eurjchem-228	56	4	.	.	PUNCT
eurjchem-228	57	1	ft‐ir	ft‐ir	NOUN
eurjchem-228	57	2	(	(	PUNCT
eurjchem-228	57	3	kbr	kbr	PROPN
eurjchem-228	57	4	,	,	PUNCT
eurjchem-228	57	5	cm‐1	cm‐1	PROPN
eurjchem-228	57	6	):	):	PUNCT
eurjchem-228	57	7	3252	3252	NUM
eurjchem-228	57	8	(	(	PUNCT
eurjchem-228	57	9	nh	nh	NOUN
eurjchem-228	57	10	)	)	PUNCT
eurjchem-228	57	11	,	,	PUNCT
eurjchem-228	57	12	1625	1625	NUM
eurjchem-228	57	13	(	(	PUNCT
eurjchem-228	57	14	co	co	NOUN
eurjchem-228	57	15	)	)	PUNCT
eurjchem-228	57	16	.	.	PUNCT
eurjchem-228	58	1	1h	1h	NUM
eurjchem-228	58	2	nmr	nmr	NOUN
eurjchem-228	58	3	(	(	PUNCT
eurjchem-228	58	4	400	400	NUM
eurjchem-228	58	5	mhz	mhz	NOUN
eurjchem-228	58	6	,	,	PUNCT
eurjchem-228	58	7	dmso‐d6	dmso‐d6	NUM
eurjchem-228	58	8	):	):	PUNCT
eurjchem-228	58	9	2.88	2.88	NUM
eurjchem-228	58	10	(	(	PUNCT
eurjchem-228	58	11	s	s	PROPN
eurjchem-228	58	12	,	,	PUNCT
eurjchem-228	58	13	3h	3h	NUM
eurjchem-228	58	14	,	,	PUNCT
eurjchem-228	58	15	ch3	ch3	PROPN
eurjchem-228	58	16	)	)	PUNCT
eurjchem-228	58	17	,	,	PUNCT
eurjchem-228	58	18	3.03	3.03	NUM
eurjchem-228	58	19	(	(	PUNCT
eurjchem-228	58	20	s	s	PROPN
eurjchem-228	58	21	,	,	PUNCT
eurjchem-228	58	22	3h	3h	NUM
eurjchem-228	58	23	,	,	PUNCT
eurjchem-228	58	24	ch3	ch3	PROPN
eurjchem-228	58	25	)	)	PUNCT
eurjchem-228	58	26	,	,	PUNCT
eurjchem-228	58	27	5.62	5.62	NUM
eurjchem-228	58	28	(	(	PUNCT
eurjchem-228	58	29	d	d	PROPN
eurjchem-228	58	30	,	,	PUNCT
eurjchem-228	58	31	1h	1h	NUM
eurjchem-228	58	32	,	,	PUNCT
eurjchem-228	58	33	j=12.4	j=12.4	PROPN
eurjchem-228	58	34	hz	hz	NOUN
eurjchem-228	58	35	,	,	PUNCT
eurjchem-228	58	36	ch	ch	NOUN
eurjchem-228	58	37	)	)	PUNCT
eurjchem-228	58	38	,	,	PUNCT
eurjchem-228	58	39	6.08‐6.10	6.08‐6.10	NUM
eurjchem-228	58	40	(	(	PUNCT
eurjchem-228	58	41	m	m	PROPN
eurjchem-228	58	42	,	,	PUNCT
eurjchem-228	58	43	1h	1h	NUM
eurjchem-228	58	44	,	,	PUNCT
eurjchem-228	58	45	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	58	46	)	)	PUNCT
eurjchem-228	58	47	,	,	PUNCT
eurjchem-228	58	48	6.76‐6.78	6.76‐6.78	NUM
eurjchem-228	58	49	(	(	PUNCT
eurjchem-228	58	50	m	m	PROPN
eurjchem-228	58	51	,	,	PUNCT
eurjchem-228	58	52	1h	1h	NUM
eurjchem-228	58	53	,	,	PUNCT
eurjchem-228	58	54	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	58	55	)	)	PUNCT
eurjchem-228	58	56	,	,	PUNCT
eurjchem-228	58	57	6.86‐6.88	6.86‐6.88	NUM
eurjchem-228	58	58	(	(	PUNCT
eurjchem-228	58	59	m	m	PROPN
eurjchem-228	58	60	,	,	PUNCT
eurjchem-228	58	61	1h	1h	NUM
eurjchem-228	58	62	,	,	PUNCT
eurjchem-228	58	63	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	58	64	)	)	PUNCT
eurjchem-228	58	65	,	,	PUNCT
eurjchem-228	58	66	7.68	7.68	NUM
eurjchem-228	58	67	(	(	PUNCT
eurjchem-228	58	68	d	d	PROPN
eurjchem-228	58	69	,	,	PUNCT
eurjchem-228	58	70	1h	1h	NUM
eurjchem-228	58	71	,	,	PUNCT
eurjchem-228	58	72	j=12.4	j=12.4	PROPN
eurjchem-228	58	73	hz	hz	NOUN
eurjchem-228	58	74	,	,	PUNCT
eurjchem-228	58	75	ch	ch	NOUN
eurjchem-228	58	76	)	)	PUNCT
eurjchem-228	58	77	,	,	PUNCT
eurjchem-228	58	78	11.41	11.41	NUM
eurjchem-228	58	79	(	(	PUNCT
eurjchem-228	58	80	s	s	PROPN
eurjchem-228	58	81	,	,	PUNCT
eurjchem-228	58	82	1h	1h	NUM
eurjchem-228	58	83	,	,	PUNCT
eurjchem-228	58	84	nh	nh	PROPN
eurjchem-228	58	85	)	)	PUNCT
eurjchem-228	58	86	.	.	PUNCT
eurjchem-228	59	1	ms	ms	NOUN
eurjchem-228	59	2	(	(	PUNCT
eurjchem-228	59	3	ei	ei	PROPN
eurjchem-228	59	4	,	,	PUNCT
eurjchem-228	59	5	m	m	PROPN
eurjchem-228	59	6	/	/	SYM
eurjchem-228	59	7	z	z	NOUN
eurjchem-228	59	8	,	,	PUNCT
eurjchem-228	59	9	%	%	INTJ
eurjchem-228	59	10	):	):	PUNCT
eurjchem-228	59	11	164	164	NUM
eurjchem-228	59	12	[	[	X
eurjchem-228	59	13	m+	m+	NUM
eurjchem-228	59	14	,	,	PUNCT
eurjchem-228	59	15	100	100	NUM
eurjchem-228	59	16	%	%	NOUN
eurjchem-228	59	17	]	]	PUNCT
eurjchem-228	59	18	.	.	PUNCT
eurjchem-228	60	1	anal	anal	ADJ
eurjchem-228	60	2	.	.	PUNCT
eurjchem-228	60	3	calcd	calcd	NOUN
eurjchem-228	60	4	.	.	PUNCT
eurjchem-228	61	1	for	for	ADP
eurjchem-228	61	2	c9h12n2o	c9h12n2o	PROPN
eurjchem-228	61	3	:	:	PUNCT
eurjchem-228	61	4	c	c	X
eurjchem-228	61	5	,	,	PUNCT
eurjchem-228	61	6	65.83	65.83	NUM
eurjchem-228	61	7	;	;	PUNCT
eurjchem-228	61	8	h	h	NOUN
eurjchem-228	61	9	,	,	PUNCT
eurjchem-228	61	10	7.37	7.37	NUM
eurjchem-228	61	11	;	;	PUNCT
eurjchem-228	61	12	n	n	CCONJ
eurjchem-228	61	13	,	,	PUNCT
eurjchem-228	61	14	17.06	17.06	NUM
eurjchem-228	61	15	.	.	PUNCT
eurjchem-228	62	1	found	find	VERB
eurjchem-228	62	2	:	:	PUNCT
eurjchem-228	63	1	c	c	X
eurjchem-228	63	2	,	,	PUNCT
eurjchem-228	63	3	65.82	65.82	NUM
eurjchem-228	63	4	;	;	PUNCT
eurjchem-228	63	5	h	h	NOUN
eurjchem-228	63	6	,	,	PUNCT
eurjchem-228	63	7	7.91	7.91	NUM
eurjchem-228	63	8	;	;	PUNCT
eurjchem-228	63	9	n	n	CCONJ
eurjchem-228	63	10	,	,	PUNCT
eurjchem-228	63	11	17.06	17.06	NUM
eurjchem-228	63	12	.	.	PUNCT
eurjchem-228	64	1	3‐dimethylamino‐1‐phenyl‐propenone	3‐dimethylamino‐1‐phenyl‐propenone	NUM
eurjchem-228	64	2	,	,	PUNCT
eurjchem-228	64	3	2c	2c	NUM
eurjchem-228	64	4	:	:	PUNCT
eurjchem-228	64	5	orange	orange	ADJ
eurjchem-228	64	6	crystals	crystal	NOUN
eurjchem-228	64	7	.	.	PUNCT
eurjchem-228	65	1	yield	yield	NOUN
eurjchem-228	65	2	:	:	PUNCT
eurjchem-228	65	3	87	87	NUM
eurjchem-228	65	4	%	%	NOUN
eurjchem-228	65	5	.	.	PUNCT
eurjchem-228	66	1	ft‐ir	ft‐ir	NOUN
eurjchem-228	66	2	(	(	PUNCT
eurjchem-228	66	3	kbr	kbr	PROPN
eurjchem-228	66	4	,	,	PUNCT
eurjchem-228	66	5	cm‐1	cm‐1	PROPN
eurjchem-228	66	6	):	):	PUNCT
eurjchem-228	66	7	1639	1639	NUM
eurjchem-228	66	8	(	(	PUNCT
eurjchem-228	66	9	co	co	NOUN
eurjchem-228	66	10	)	)	PUNCT
eurjchem-228	66	11	.	.	PUNCT
eurjchem-228	67	1	1h	1h	NUM
eurjchem-228	67	2	nmr	nmr	NOUN
eurjchem-228	67	3	(	(	PUNCT
eurjchem-228	67	4	400	400	NUM
eurjchem-228	67	5	mhz	mhz	NOUN
eurjchem-228	67	6	,	,	PUNCT
eurjchem-228	67	7	dmso‐d6	dmso‐d6	NUM
eurjchem-228	67	8	):	):	PUNCT
eurjchem-228	67	9	2.90	2.90	NUM
eurjchem-228	67	10	(	(	PUNCT
eurjchem-228	67	11	s	s	PROPN
eurjchem-228	67	12	,	,	PUNCT
eurjchem-228	67	13	3h	3h	NUM
eurjchem-228	67	14	,	,	PUNCT
eurjchem-228	67	15	ch3	ch3	PROPN
eurjchem-228	67	16	)	)	PUNCT
eurjchem-228	67	17	,	,	PUNCT
eurjchem-228	67	18	3.14	3.14	NUM
eurjchem-228	67	19	(	(	PUNCT
eurjchem-228	67	20	s	s	PROPN
eurjchem-228	67	21	,	,	PUNCT
eurjchem-228	67	22	3h	3h	NUM
eurjchem-228	67	23	,	,	PUNCT
eurjchem-228	67	24	ch3	ch3	PROPN
eurjchem-228	67	25	)	)	PUNCT
eurjchem-228	67	26	,	,	PUNCT
eurjchem-228	67	27	5.81	5.81	NUM
eurjchem-228	67	28	(	(	PUNCT
eurjchem-228	67	29	d	d	PROPN
eurjchem-228	67	30	,	,	PUNCT
eurjchem-228	67	31	1h	1h	NUM
eurjchem-228	67	32	,	,	PUNCT
eurjchem-228	67	33	j=12.4	j=12.4	PROPN
eurjchem-228	67	34	hz	hz	NOUN
eurjchem-228	67	35	,	,	PUNCT
eurjchem-228	67	36	ch	ch	NOUN
eurjchem-228	67	37	)	)	PUNCT
eurjchem-228	67	38	,	,	PUNCT
eurjchem-228	67	39	7.41‐7.50	7.41‐7.50	NUM
eurjchem-228	67	40	(	(	PUNCT
eurjchem-228	67	41	m	m	PROPN
eurjchem-228	67	42	,	,	PUNCT
eurjchem-228	67	43	3h	3h	NUM
eurjchem-228	67	44	,	,	PUNCT
eurjchem-228	67	45	phenyl‐h	phenyl‐h	NOUN
eurjchem-228	67	46	)	)	PUNCT
eurjchem-228	67	47	,	,	PUNCT
eurjchem-228	67	48	7.70	7.70	NUM
eurjchem-228	67	49	(	(	PUNCT
eurjchem-228	67	50	d	d	PROPN
eurjchem-228	67	51	,	,	PUNCT
eurjchem-228	67	52	1h	1h	NUM
eurjchem-228	67	53	,	,	PUNCT
eurjchem-228	67	54	j=12.4	j=12.4	PROPN
eurjchem-228	67	55	hz	hz	NOUN
eurjchem-228	67	56	,	,	PUNCT
eurjchem-228	67	57	ch	ch	NOUN
eurjchem-228	67	58	)	)	PUNCT
eurjchem-228	67	59	,	,	PUNCT
eurjchem-228	67	60	7.88‐7.90	7.88‐7.90	NUM
eurjchem-228	67	61	(	(	PUNCT
eurjchem-228	67	62	m	m	PROPN
eurjchem-228	67	63	,	,	PUNCT
eurjchem-228	67	64	2h	2h	NUM
eurjchem-228	67	65	,	,	PUNCT
eurjchem-228	67	66	phenyl‐h	phenyl‐h	NOUN
eurjchem-228	67	67	)	)	PUNCT
eurjchem-228	67	68	.	.	PUNCT
eurjchem-228	68	1	ms	ms	NOUN
eurjchem-228	68	2	(	(	PUNCT
eurjchem-228	68	3	ei	ei	PROPN
eurjchem-228	68	4	,	,	PUNCT
eurjchem-228	68	5	m	m	PROPN
eurjchem-228	68	6	/	/	SYM
eurjchem-228	68	7	z	z	NOUN
eurjchem-228	68	8	,	,	PUNCT
eurjchem-228	68	9	%	%	INTJ
eurjchem-228	68	10	):	):	PUNCT
eurjchem-228	68	11	175	175	NUM
eurjchem-228	68	12	[	[	X
eurjchem-228	68	13	m+	m+	NUM
eurjchem-228	68	14	,	,	PUNCT
eurjchem-228	68	15	89	89	NUM
eurjchem-228	68	16	%	%	NOUN
eurjchem-228	68	17	]	]	PUNCT
eurjchem-228	68	18	.	.	PUNCT
eurjchem-228	69	1	2‐(1‐dimethylaminomethylene‐2‐oxo‐propyl)isoindole‐1,3‐	2‐(1‐dimethylaminomethylene‐2‐oxo‐propyl)isoindole‐1,3‐	NUM
eurjchem-228	69	2	dione	dione	NOUN
eurjchem-228	69	3	,	,	PUNCT
eurjchem-228	69	4	3	3	NUM
eurjchem-228	69	5	:	:	PUNCT
eurjchem-228	69	6	light	light	ADJ
eurjchem-228	69	7	yellow	yellow	ADJ
eurjchem-228	69	8	crystals	crystal	NOUN
eurjchem-228	69	9	.	.	PUNCT
eurjchem-228	70	1	yield	yield	NOUN
eurjchem-228	70	2	:	:	PUNCT
eurjchem-228	70	3	15	15	NUM
eurjchem-228	70	4	%	%	NOUN
eurjchem-228	70	5	.	.	PUNCT
eurjchem-228	71	1	m.p	m.p	PROPN
eurjchem-228	71	2	.	.	PROPN
eurjchem-228	71	3	:	:	PUNCT
eurjchem-228	72	1	176‐178	176‐178	NUM
eurjchem-228	72	2	°	°	NUM
eurjchem-228	72	3	c	c	VERB
eurjchem-228	72	4	.	.	PUNCT
eurjchem-228	73	1	ft‐	ft‐	PROPN
eurjchem-228	73	2	ir	ir	PROPN
eurjchem-228	73	3	(	(	PUNCT
eurjchem-228	73	4	kbr	kbr	PROPN
eurjchem-228	73	5	,	,	PUNCT
eurjchem-228	73	6	cm‐1	cm‐1	PROPN
eurjchem-228	73	7	):	):	PUNCT
eurjchem-228	73	8	1771	1771	NUM
eurjchem-228	73	9	,	,	PUNCT
eurjchem-228	73	10	1715	1715	NUM
eurjchem-228	73	11	,	,	PUNCT
eurjchem-228	73	12	1653	1653	NUM
eurjchem-228	73	13	(	(	PUNCT
eurjchem-228	73	14	co	co	NOUN
eurjchem-228	73	15	)	)	PUNCT
eurjchem-228	73	16	.	.	PUNCT
eurjchem-228	74	1	1h	1h	NUM
eurjchem-228	74	2	nmr	nmr	NOUN
eurjchem-228	74	3	(	(	PUNCT
eurjchem-228	74	4	400	400	NUM
eurjchem-228	74	5	mhz	mhz	NOUN
eurjchem-228	74	6	,	,	PUNCT
eurjchem-228	74	7	cdcl3	cdcl3	NOUN
eurjchem-228	74	8	):	):	PUNCT
eurjchem-228	74	9	2.91	2.91	NUM
eurjchem-228	74	10	(	(	PUNCT
eurjchem-228	74	11	s	s	PROPN
eurjchem-228	74	12	,	,	PUNCT
eurjchem-228	74	13	3h	3h	NUM
eurjchem-228	74	14	,	,	PUNCT
eurjchem-228	74	15	ch3	ch3	PROPN
eurjchem-228	74	16	)	)	PUNCT
eurjchem-228	74	17	,	,	PUNCT
eurjchem-228	74	18	2.98	2.98	NUM
eurjchem-228	74	19	(	(	PUNCT
eurjchem-228	74	20	s	s	PROPN
eurjchem-228	74	21	,	,	PUNCT
eurjchem-228	74	22	3h	3h	NUM
eurjchem-228	74	23	,	,	PUNCT
eurjchem-228	74	24	nch3	nch3	PROPN
eurjchem-228	74	25	)	)	PUNCT
eurjchem-228	74	26	,	,	PUNCT
eurjchem-228	74	27	3.22	3.22	NUM
eurjchem-228	74	28	(	(	PUNCT
eurjchem-228	74	29	s	s	PROPN
eurjchem-228	74	30	,	,	PUNCT
eurjchem-228	74	31	3h	3h	NUM
eurjchem-228	74	32	,	,	PUNCT
eurjchem-228	74	33	nch3	nch3	PROPN
eurjchem-228	74	34	)	)	PUNCT
eurjchem-228	74	35	,	,	PUNCT
eurjchem-228	74	36	7.72‐7.75	7.72‐7.75	NUM
eurjchem-228	74	37	(	(	PUNCT
eurjchem-228	74	38	m	m	PROPN
eurjchem-228	74	39	,	,	PUNCT
eurjchem-228	74	40	2h	2h	NUM
eurjchem-228	74	41	,	,	PUNCT
eurjchem-228	74	42	phthalimidyl‐h	phthalimidyl‐h	NOUN
eurjchem-228	74	43	)	)	PUNCT
eurjchem-228	74	44	,	,	PUNCT
eurjchem-228	74	45	7.79	7.79	NUM
eurjchem-228	74	46	(	(	PUNCT
eurjchem-228	74	47	s	s	PROPN
eurjchem-228	74	48	,	,	PUNCT
eurjchem-228	74	49	1h	1h	NUM
eurjchem-228	74	50	,	,	PUNCT
eurjchem-228	74	51	ch	ch	NOUN
eurjchem-228	74	52	)	)	PUNCT
eurjchem-228	74	53	,	,	PUNCT
eurjchem-228	74	54	7.87‐7.90	7.87‐7.90	NUM
eurjchem-228	74	55	(	(	PUNCT
eurjchem-228	74	56	m	m	PROPN
eurjchem-228	74	57	,	,	PUNCT
eurjchem-228	74	58	2h	2h	NUM
eurjchem-228	74	59	,	,	PUNCT
eurjchem-228	74	60	phthalimidyl‐h	phthalimidyl‐h	NOUN
eurjchem-228	74	61	)	)	PUNCT
eurjchem-228	74	62	.	.	PUNCT
eurjchem-228	75	1	ms	ms	NOUN
eurjchem-228	75	2	(	(	PUNCT
eurjchem-228	75	3	ei	ei	PROPN
eurjchem-228	75	4	,	,	PUNCT
eurjchem-228	75	5	m	m	PROPN
eurjchem-228	75	6	/	/	SYM
eurjchem-228	75	7	z	z	NOUN
eurjchem-228	75	8	,	,	PUNCT
eurjchem-228	75	9	%	%	INTJ
eurjchem-228	75	10	):	):	PUNCT
eurjchem-228	75	11	258	258	NUM
eurjchem-228	76	1	[	[	X
eurjchem-228	76	2	m+	m+	NUM
eurjchem-228	76	3	,	,	PUNCT
eurjchem-228	76	4	8	8	NUM
eurjchem-228	76	5	%	%	NOUN
eurjchem-228	76	6	]	]	PUNCT
eurjchem-228	76	7	.	.	PUNCT
eurjchem-228	77	1	anal	anal	ADJ
eurjchem-228	77	2	.	.	PUNCT
eurjchem-228	77	3	calcd	calcd	NOUN
eurjchem-228	77	4	.	.	PUNCT
eurjchem-228	78	1	for	for	ADP
eurjchem-228	78	2	c14h14n2o3	c14h14n2o3	NOUN
eurjchem-228	78	3	:	:	PUNCT
eurjchem-228	78	4	c	c	X
eurjchem-228	78	5	,	,	PUNCT
eurjchem-228	78	6	65.11	65.11	NUM
eurjchem-228	78	7	;	;	PUNCT
eurjchem-228	78	8	h	h	X
eurjchem-228	78	9	,	,	PUNCT
eurjchem-228	78	10	5.46	5.46	NUM
eurjchem-228	78	11	;	;	PUNCT
eurjchem-228	78	12	n	n	CCONJ
eurjchem-228	78	13	,	,	PUNCT
eurjchem-228	78	14	10.85	10.85	NUM
eurjchem-228	78	15	.	.	PUNCT
eurjchem-228	78	16	found	find	VERB
eurjchem-228	78	17	:	:	PUNCT
eurjchem-228	79	1	c	c	X
eurjchem-228	79	2	,	,	PUNCT
eurjchem-228	79	3	65.01	65.01	NUM
eurjchem-228	79	4	;	;	PUNCT
eurjchem-228	79	5	h	h	NOUN
eurjchem-228	79	6	,	,	PUNCT
eurjchem-228	79	7	5.61	5.61	NUM
eurjchem-228	79	8	;	;	PUNCT
eurjchem-228	79	9	n	n	CCONJ
eurjchem-228	79	10	,	,	PUNCT
eurjchem-228	79	11	11.05	11.05	NUM
eurjchem-228	79	12	.	.	PUNCT
eurjchem-228	80	1	2.3	2.3	NUM
eurjchem-228	80	2	.	.	PUNCT
eurjchem-228	80	3	synthesis	synthesis	NOUN
eurjchem-228	80	4	of	of	ADP
eurjchem-228	80	5	compounds	compound	NOUN
eurjchem-228	80	6	(	(	PUNCT
eurjchem-228	80	7	6a	6a	NOUN
eurjchem-228	80	8	,	,	PUNCT
eurjchem-228	80	9	b	b	NOUN
eurjchem-228	80	10	)	)	PUNCT
eurjchem-228	80	11	2.3.1	2.3.1	NUM
eurjchem-228	80	12	.	.	PUNCT
eurjchem-228	81	1	2‐(2‐3,5‐di[2‐(1,3‐dioxo‐2,3‐dihydro‐1h‐2‐isoindolyl	2‐(2‐3,5‐di[2‐(1,3‐dioxo‐2,3‐dihydro‐1h‐2‐isoindolyl	NUM
eurjchem-228	81	2	)	)	PUNCT
eurjchem-228	81	3	acetyl]phenyl‐2‐oxoethyl)‐1,3‐isoindolinedione	acetyl]phenyl‐2‐oxoethyl)‐1,3‐isoindolinedione	NOUN
eurjchem-228	81	4	(	(	PUNCT
eurjchem-228	81	5	6a	6a	NOUN
eurjchem-228	81	6	)	)	PUNCT
eurjchem-228	81	7	a	a	DET
eurjchem-228	81	8	mixture	mixture	NOUN
eurjchem-228	81	9	of	of	ADP
eurjchem-228	81	10	compound	compound	NOUN
eurjchem-228	81	11	2a	2a	NUM
eurjchem-228	81	12	(	(	PUNCT
eurjchem-228	81	13	2.58	2.58	NUM
eurjchem-228	81	14	g	g	NOUN
eurjchem-228	81	15	,	,	PUNCT
eurjchem-228	81	16	0.01	0.01	NUM
eurjchem-228	81	17	mol	mol	NOUN
eurjchem-228	81	18	)	)	PUNCT
eurjchem-228	81	19	,	,	PUNCT
eurjchem-228	81	20	indium	indium	NOUN
eurjchem-228	81	21	chloride	chloride	NOUN
eurjchem-228	81	22	(	(	PUNCT
eurjchem-228	81	23	0.02	0.02	NUM
eurjchem-228	81	24	g	g	NOUN
eurjchem-228	81	25	)	)	PUNCT
eurjchem-228	81	26	and	and	CCONJ
eurjchem-228	81	27	acetic	acetic	ADJ
eurjchem-228	81	28	acid	acid	NOUN
eurjchem-228	81	29	(	(	PUNCT
eurjchem-228	81	30	0.5	0.5	NUM
eurjchem-228	81	31	ml	ml	NOUN
eurjchem-228	81	32	)	)	PUNCT
eurjchem-228	81	33	was	be	AUX
eurjchem-228	81	34	irradiated	irradiate	VERB
eurjchem-228	81	35	in	in	ADP
eurjchem-228	81	36	microwave	microwave	NOUN
eurjchem-228	81	37	at	at	ADP
eurjchem-228	81	38	140	140	NUM
eurjchem-228	81	39	oc	oc	NOUN
eurjchem-228	81	40	for	for	ADP
eurjchem-228	81	41	30	30	NUM
eurjchem-228	81	42	min	min	NOUN
eurjchem-228	81	43	.	.	PUNCT
eurjchem-228	82	1	the	the	DET
eurjchem-228	82	2	crude	crude	ADJ
eurjchem-228	82	3	product	product	NOUN
eurjchem-228	82	4	was	be	AUX
eurjchem-228	82	5	poured	pour	VERB
eurjchem-228	82	6	onto	onto	ADP
eurjchem-228	82	7	water	water	NOUN
eurjchem-228	82	8	,	,	PUNCT
eurjchem-228	82	9	the	the	DET
eurjchem-228	82	10	solid	solid	ADJ
eurjchem-228	82	11	product	product	NOUN
eurjchem-228	82	12	,	,	PUNCT
eurjchem-228	82	13	so	so	ADV
eurjchem-228	82	14	formed	form	VERB
eurjchem-228	82	15	,	,	PUNCT
eurjchem-228	82	16	was	be	AUX
eurjchem-228	82	17	collected	collect	VERB
eurjchem-228	82	18	by	by	ADP
eurjchem-228	82	19	filtration	filtration	NOUN
eurjchem-228	82	20	and	and	CCONJ
eurjchem-228	82	21	crystallized	crystallize	VERB
eurjchem-228	82	22	from	from	ADP
eurjchem-228	82	23	toluene	toluene	NOUN
eurjchem-228	82	24	.	.	PUNCT
eurjchem-228	83	1	light	light	ADJ
eurjchem-228	83	2	brown	brown	PROPN
eurjchem-228	83	3	.	.	PUNCT
eurjchem-228	84	1	yield	yield	NOUN
eurjchem-228	84	2	:	:	PUNCT
eurjchem-228	84	3	58	58	NUM
eurjchem-228	84	4	%	%	NOUN
eurjchem-228	84	5	.	.	PUNCT
eurjchem-228	85	1	m.p	m.p	PROPN
eurjchem-228	85	2	.	.	PROPN
eurjchem-228	85	3	:	:	PUNCT
eurjchem-228	86	1	300‐301	300‐301	NUM
eurjchem-228	86	2	oc	oc	NOUN
eurjchem-228	86	3	.	.	PUNCT
eurjchem-228	86	4	ft‐ir	ft‐ir	NOUN
eurjchem-228	86	5	(	(	PUNCT
eurjchem-228	86	6	kbr	kbr	PROPN
eurjchem-228	86	7	,	,	PUNCT
eurjchem-228	86	8	cm‐1	cm‐1	PROPN
eurjchem-228	86	9	):	):	PUNCT
eurjchem-228	86	10	1776	1776	NUM
eurjchem-228	86	11	,	,	PUNCT
eurjchem-228	86	12	1721	1721	NUM
eurjchem-228	86	13	(	(	PUNCT
eurjchem-228	86	14	co	co	NOUN
eurjchem-228	86	15	)	)	PUNCT
eurjchem-228	86	16	.	.	PUNCT
eurjchem-228	87	1	1h	1h	NUM
eurjchem-228	87	2	nmr	nmr	NOUN
eurjchem-228	87	3	(	(	PUNCT
eurjchem-228	87	4	400	400	NUM
eurjchem-228	87	5	mhz	mhz	NOUN
eurjchem-228	87	6	,	,	PUNCT
eurjchem-228	87	7	dmso‐d6	dmso‐d6	NUM
eurjchem-228	87	8	):	):	PUNCT
eurjchem-228	87	9	5.57	5.57	NUM
eurjchem-228	87	10	(	(	PUNCT
eurjchem-228	87	11	s	s	PROPN
eurjchem-228	87	12	,	,	PUNCT
eurjchem-228	87	13	6h	6h	NUM
eurjchem-228	87	14	,	,	PUNCT
eurjchem-228	87	15	ch2	ch2	PROPN
eurjchem-228	87	16	)	)	PUNCT
eurjchem-228	87	17	,	,	PUNCT
eurjchem-228	87	18	7.93‐7.99	7.93‐7.99	NUM
eurjchem-228	87	19	(	(	PUNCT
eurjchem-228	87	20	m‐12h	m‐12h	PROPN
eurjchem-228	87	21	,	,	PUNCT
eurjchem-228	87	22	phthal‐imidyl‐h	phthal‐imidyl‐h	PROPN
eurjchem-228	87	23	)	)	PUNCT
eurjchem-228	87	24	,	,	PUNCT
eurjchem-228	87	25	8.98	8.98	NUM
eurjchem-228	87	26	(	(	PUNCT
eurjchem-228	87	27	s	s	PROPN
eurjchem-228	87	28	,	,	PUNCT
eurjchem-228	87	29	3h	3h	NUM
eurjchem-228	87	30	,	,	PUNCT
eurjchem-228	87	31	benzyl‐h	benzyl‐h	NOUN
eurjchem-228	87	32	)	)	PUNCT
eurjchem-228	87	33	.	.	PUNCT
eurjchem-228	88	1	13c	13c	NOUN
eurjchem-228	88	2	nmr	nmr	NOUN
eurjchem-228	88	3	(	(	PUNCT
eurjchem-228	88	4	dmso‐d6	dmso‐d6	NOUN
eurjchem-228	88	5	):	):	PUNCT
eurjchem-228	88	6	192.23	192.23	NUM
eurjchem-228	88	7	,	,	PUNCT
eurjchem-228	88	8	167.98	167.98	NUM
eurjchem-228	88	9	(	(	PUNCT
eurjchem-228	88	10	2	2	NUM
eurjchem-228	88	11	co	co	NOUN
eurjchem-228	88	12	)	)	PUNCT
eurjchem-228	88	13	,	,	PUNCT
eurjchem-228	88	14	135.33	135.33	NUM
eurjchem-228	88	15	,	,	PUNCT
eurjchem-228	88	16	135.20	135.20	NUM
eurjchem-228	88	17	,	,	PUNCT
eurjchem-228	88	18	133.39	133.39	NUM
eurjchem-228	88	19	,	,	PUNCT
eurjchem-228	88	20	132.02	132.02	NUM
eurjchem-228	88	21	,	,	PUNCT
eurjchem-228	88	22	123.93	123.93	NUM
eurjchem-228	88	23	,	,	PUNCT
eurjchem-228	88	24	45.50	45.50	NUM
eurjchem-228	88	25	(	(	PUNCT
eurjchem-228	88	26	ch2	ch2	PROPN
eurjchem-228	88	27	)	)	PUNCT
eurjchem-228	88	28	.	.	PUNCT
eurjchem-228	89	1	ms	ms	NOUN
eurjchem-228	89	2	(	(	PUNCT
eurjchem-228	89	3	ei	ei	PROPN
eurjchem-228	89	4	,	,	PUNCT
eurjchem-228	89	5	m	m	PROPN
eurjchem-228	89	6	/	/	SYM
eurjchem-228	89	7	z	z	NOUN
eurjchem-228	89	8	,	,	PUNCT
eurjchem-228	89	9	%	%	INTJ
eurjchem-228	89	10	):	):	PUNCT
eurjchem-228	89	11	639	639	NUM
eurjchem-228	90	1	[	[	X
eurjchem-228	90	2	m+	m+	NUM
eurjchem-228	90	3	,	,	PUNCT
eurjchem-228	90	4	12	12	NUM
eurjchem-228	90	5	%	%	NOUN
eurjchem-228	90	6	]	]	PUNCT
eurjchem-228	90	7	.	.	PUNCT
eurjchem-228	91	1	anal	anal	PROPN
eurjchem-228	91	2	.	.	PUNCT
eurjchem-228	91	3	calcd	calcd	NOUN
eurjchem-228	91	4	.	.	PUNCT
eurjchem-228	92	1	for	for	ADP
eurjchem-228	92	2	c36h21	c36h21	PROPN
eurjchem-228	92	3	n3o9	n3o9	SYM
eurjchem-228	92	4	:	:	PUNCT
eurjchem-228	92	5	c	c	X
eurjchem-228	92	6	,	,	PUNCT
eurjchem-228	92	7	67.61	67.61	NUM
eurjchem-228	92	8	;	;	PUNCT
eurjchem-228	92	9	h	h	NOUN
eurjchem-228	92	10	,	,	PUNCT
eurjchem-228	92	11	3.31	3.31	NUM
eurjchem-228	92	12	;	;	PUNCT
eurjchem-228	92	13	n	n	CCONJ
eurjchem-228	92	14	,	,	PUNCT
eurjchem-228	92	15	6.57	6.57	NUM
eurjchem-228	92	16	.	.	PUNCT
eurjchem-228	92	17	found	find	VERB
eurjchem-228	92	18	67.46	67.46	NUM
eurjchem-228	92	19	;	;	PUNCT
eurjchem-228	92	20	h	h	NOUN
eurjchem-228	92	21	,	,	PUNCT
eurjchem-228	92	22	3.33	3.33	NUM
eurjchem-228	92	23	;	;	PUNCT
eurjchem-228	92	24	n	n	CCONJ
eurjchem-228	92	25	,	,	PUNCT
eurjchem-228	92	26	6.81	6.81	NUM
eurjchem-228	92	27	.	.	PUNCT
eurjchem-228	93	1	2.3.2	2.3.2	NUM
eurjchem-228	93	2	.	.	PUNCT
eurjchem-228	94	1	[	[	X
eurjchem-228	94	2	3,5‐di(1h‐2‐pyrrolylcarbonyl)phenyl](1h‐2‐pyrrolyl	3,5‐di(1h‐2‐pyrrolylcarbonyl)phenyl](1h‐2‐pyrrolyl	NUM
eurjchem-228	94	3	)	)	PUNCT
eurjchem-228	94	4	methanone	methanone	NOUN
eurjchem-228	94	5	(	(	PUNCT
eurjchem-228	94	6	6b	6b	NOUN
eurjchem-228	94	7	)	)	PUNCT
eurjchem-228	94	8	a	a	DET
eurjchem-228	94	9	mixture	mixture	NOUN
eurjchem-228	94	10	of	of	ADP
eurjchem-228	94	11	compound	compound	NOUN
eurjchem-228	94	12	2b	2b	NOUN
eurjchem-228	94	13	(	(	PUNCT
eurjchem-228	94	14	1.64	1.64	NUM
eurjchem-228	94	15	g	g	NOUN
eurjchem-228	94	16	,	,	PUNCT
eurjchem-228	94	17	0.01	0.01	NUM
eurjchem-228	94	18	mol	mol	NOUN
eurjchem-228	94	19	)	)	PUNCT
eurjchem-228	94	20	and	and	CCONJ
eurjchem-228	94	21	acetic	acetic	ADJ
eurjchem-228	94	22	acid	acid	NOUN
eurjchem-228	94	23	(	(	PUNCT
eurjchem-228	94	24	0.5	0.5	NUM
eurjchem-228	94	25	ml	ml	NOUN
eurjchem-228	94	26	)	)	PUNCT
eurjchem-228	94	27	was	be	AUX
eurjchem-228	94	28	irradiated	irradiate	VERB
eurjchem-228	94	29	by	by	ADP
eurjchem-228	94	30	focused	focused	ADJ
eurjchem-228	94	31	microwave	microwave	NOUN
eurjchem-228	94	32	at	at	ADP
eurjchem-228	94	33	140	140	NUM
eurjchem-228	94	34	°	°	ADP
eurjchem-228	94	35	c	c	NOUN
eurjchem-228	94	36	for	for	ADP
eurjchem-228	94	37	30	30	NUM
eurjchem-228	94	38	min	min	NOUN
eurjchem-228	94	39	.	.	NOUN
eurjchem-228	94	40	completion	completion	NOUN
eurjchem-228	94	41	of	of	ADP
eurjchem-228	94	42	reaction	reaction	NOUN
eurjchem-228	94	43	was	be	AUX
eurjchem-228	94	44	monitored	monitor	VERB
eurjchem-228	94	45	by	by	ADP
eurjchem-228	94	46	tlc	tlc	PROPN
eurjchem-228	94	47	.	.	PUNCT
eurjchem-228	95	1	the	the	DET
eurjchem-228	95	2	solid	solid	ADJ
eurjchem-228	95	3	product	product	NOUN
eurjchem-228	95	4	,	,	PUNCT
eurjchem-228	95	5	so	so	ADV
eurjchem-228	95	6	formed	form	VERB
eurjchem-228	95	7	,	,	PUNCT
eurjchem-228	95	8	was	be	AUX
eurjchem-228	95	9	collected	collect	VERB
eurjchem-228	95	10	and	and	CCONJ
eurjchem-228	95	11	crystallized	crystallize	VERB
eurjchem-228	95	12	from	from	ADP
eurjchem-228	95	13	dioxane	dioxane	NOUN
eurjchem-228	95	14	to	to	PART
eurjchem-228	95	15	afford	afford	VERB
eurjchem-228	95	16	compounds	compound	NOUN
eurjchem-228	95	17	6b	6b	NUM
eurjchem-228	95	18	.	.	PUNCT
eurjchem-228	96	1	yield	yield	VERB
eurjchem-228	96	2	93	93	NUM
eurjchem-228	96	3	%	%	NOUN
eurjchem-228	96	4	.	.	PUNCT
eurjchem-228	97	1	m.p	m.p	PROPN
eurjchem-228	97	2	.	.	PROPN
eurjchem-228	97	3	:	:	PUNCT
eurjchem-228	98	1	259‐260	259‐260	NUM
eurjchem-228	98	2	°	°	ADP
eurjchem-228	98	3	c	c	NOUN
eurjchem-228	98	4	.	.	PUNCT
eurjchem-228	98	5	ft‐ir	ft‐ir	NOUN
eurjchem-228	98	6	(	(	PUNCT
eurjchem-228	98	7	kbr	kbr	PROPN
eurjchem-228	98	8	,	,	PUNCT
eurjchem-228	98	9	cm‐1	cm‐1	PROPN
eurjchem-228	98	10	):	):	PUNCT
eurjchem-228	98	11	3290	3290	NUM
eurjchem-228	98	12	(	(	PUNCT
eurjchem-228	98	13	nh	nh	NOUN
eurjchem-228	98	14	)	)	PUNCT
eurjchem-228	98	15	,	,	PUNCT
eurjchem-228	98	16	1626	1626	NUM
eurjchem-228	98	17	(	(	PUNCT
eurjchem-228	98	18	co	co	NOUN
eurjchem-228	98	19	)	)	PUNCT
eurjchem-228	98	20	.	.	PUNCT
eurjchem-228	99	1	1h	1h	NUM
eurjchem-228	99	2	nmr	nmr	NOUN
eurjchem-228	99	3	(	(	PUNCT
eurjchem-228	99	4	400	400	NUM
eurjchem-228	99	5	mhz	mhz	NOUN
eurjchem-228	99	6	,	,	PUNCT
eurjchem-228	99	7	dmso‐d6	dmso‐d6	NUM
eurjchem-228	99	8	):	):	PUNCT
eurjchem-228	99	9	6.130‐6.30	6.130‐6.30	NUM
eurjchem-228	99	10	(	(	PUNCT
eurjchem-228	99	11	m	m	PROPN
eurjchem-228	99	12	,	,	PUNCT
eurjchem-228	99	13	1h	1h	NUM
eurjchem-228	99	14	,	,	PUNCT
eurjchem-228	99	15	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	99	16	)	)	PUNCT
eurjchem-228	99	17	,	,	PUNCT
eurjchem-228	99	18	6.91‐6.93	6.91‐6.93	NUM
eurjchem-228	99	19	(	(	PUNCT
eurjchem-228	99	20	m	m	PROPN
eurjchem-228	99	21	,	,	PUNCT
eurjchem-228	99	22	1h	1h	NUM
eurjchem-228	99	23	,	,	PUNCT
eurjchem-228	99	24	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	99	25	)	)	PUNCT
eurjchem-228	99	26	,	,	PUNCT
eurjchem-228	99	27	7.28‐7.30	7.28‐7.30	NUM
eurjchem-228	99	28	(	(	PUNCT
eurjchem-228	99	29	m	m	PROPN
eurjchem-228	99	30	,	,	PUNCT
eurjchem-228	99	31	1h	1h	NUM
eurjchem-228	99	32	,	,	PUNCT
eurjchem-228	99	33	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	99	34	)	)	PUNCT
eurjchem-228	99	35	,	,	PUNCT
eurjchem-228	99	36	8.37	8.37	NUM
eurjchem-228	99	37	(	(	PUNCT
eurjchem-228	99	38	s	s	PROPN
eurjchem-228	99	39	,	,	PUNCT
eurjchem-228	99	40	1h	1h	NUM
eurjchem-228	99	41	,	,	PUNCT
eurjchem-228	99	42	benzoyl‐	benzoyl‐	PROPN
eurjchem-228	99	43	h	h	NOUN
eurjchem-228	99	44	)	)	PUNCT
eurjchem-228	99	45	,	,	PUNCT
eurjchem-228	99	46	12.22	12.22	NUM
eurjchem-228	99	47	(	(	PUNCT
eurjchem-228	99	48	s	s	PROPN
eurjchem-228	99	49	,	,	PUNCT
eurjchem-228	99	50	1h	1h	NUM
eurjchem-228	99	51	,	,	PUNCT
eurjchem-228	99	52	nh	nh	PROPN
eurjchem-228	99	53	)	)	PUNCT
eurjchem-228	99	54	.	.	PUNCT
eurjchem-228	100	1	13c	13c	NOUN
eurjchem-228	100	2	nmr	nmr	NOUN
eurjchem-228	100	3	(	(	PUNCT
eurjchem-228	100	4	dmso‐d6	dmso‐d6	PROPN
eurjchem-228	100	5	,	,	PUNCT
eurjchem-228	100	6	100	100	NUM
eurjchem-228	100	7	mhz	mhz	NOUN
eurjchem-228	100	8	):	):	PUNCT
eurjchem-228	100	9	182.10	182.10	NUM
eurjchem-228	100	10	(	(	PUNCT
eurjchem-228	100	11	co	co	NOUN
eurjchem-228	100	12	)	)	PUNCT
eurjchem-228	100	13	,	,	PUNCT
eurjchem-228	100	14	138.84	138.84	NUM
eurjchem-228	100	15	,	,	PUNCT
eurjchem-228	100	16	131.21	131.21	NUM
eurjchem-228	100	17	,	,	PUNCT
eurjchem-228	100	18	130.17	130.17	NUM
eurjchem-228	100	19	,	,	PUNCT
eurjchem-228	100	20	127.20	127.20	NUM
eurjchem-228	100	21	,	,	PUNCT
eurjchem-228	100	22	119.81	119.81	NUM
eurjchem-228	100	23	,	,	PUNCT
eurjchem-228	100	24	110.69	110.69	NUM
eurjchem-228	100	25	.	.	PUNCT
eurjchem-228	101	1	ms	ms	NOUN
eurjchem-228	101	2	(	(	PUNCT
eurjchem-228	101	3	ei	ei	PROPN
eurjchem-228	101	4	,	,	PUNCT
eurjchem-228	101	5	m	m	PROPN
eurjchem-228	101	6	/	/	SYM
eurjchem-228	101	7	z	z	NOUN
eurjchem-228	101	8	,	,	PUNCT
eurjchem-228	101	9	%	%	INTJ
eurjchem-228	101	10	):	):	PUNCT
eurjchem-228	101	11	357	357	NUM
eurjchem-228	101	12	[	[	X
eurjchem-228	101	13	m+	m+	NUM
eurjchem-228	101	14	,	,	PUNCT
eurjchem-228	101	15	100	100	NUM
eurjchem-228	101	16	%	%	NOUN
eurjchem-228	101	17	]	]	PUNCT
eurjchem-228	101	18	.	.	PUNCT
eurjchem-228	102	1	anal	anal	ADJ
eurjchem-228	102	2	.	.	PUNCT
eurjchem-228	102	3	calcd	calcd	NOUN
eurjchem-228	102	4	.	.	PUNCT
eurjchem-228	103	1	for	for	ADP
eurjchem-228	103	2	c21h15n3o3	c21h15n3o3	PROPN
eurjchem-228	103	3	:	:	PUNCT
eurjchem-228	103	4	c	c	X
eurjchem-228	103	5	,	,	PUNCT
eurjchem-228	103	6	70.58	70.58	NUM
eurjchem-228	103	7	;	;	PUNCT
eurjchem-228	103	8	h	h	X
eurjchem-228	103	9	,	,	PUNCT
eurjchem-228	103	10	4.23	4.23	NUM
eurjchem-228	103	11	;	;	PUNCT
eurjchem-228	103	12	n	n	CCONJ
eurjchem-228	103	13	,	,	PUNCT
eurjchem-228	103	14	11.76	11.76	NUM
eurjchem-228	103	15	.	.	PUNCT
eurjchem-228	103	16	found	find	VERB
eurjchem-228	103	17	:	:	PUNCT
eurjchem-228	104	1	c	c	X
eurjchem-228	104	2	,	,	PUNCT
eurjchem-228	104	3	69.77	69.77	NUM
eurjchem-228	104	4	;	;	PUNCT
eurjchem-228	105	1	h	h	NOUN
eurjchem-228	105	2	,	,	PUNCT
eurjchem-228	105	3	4.74	4.74	NUM
eurjchem-228	105	4	;	;	PUNCT
eurjchem-228	105	5	n	n	CCONJ
eurjchem-228	105	6	,	,	PUNCT
eurjchem-228	105	7	11.30	11.30	NUM
eurjchem-228	105	8	.	.	PUNCT
eurjchem-228	106	1	2.4	2.4	NUM
eurjchem-228	106	2	.	.	PUNCT
eurjchem-228	106	3	general	general	ADJ
eurjchem-228	106	4	procedure	procedure	NOUN
eurjchem-228	106	5	for	for	ADP
eurjchem-228	106	6	the	the	DET
eurjchem-228	106	7	synthesis	synthesis	NOUN
eurjchem-228	106	8	of	of	ADP
eurjchem-228	106	9	compounds	compound	NOUN
eurjchem-228	106	10	(	(	PUNCT
eurjchem-228	106	11	8a	8a	NUM
eurjchem-228	106	12	,	,	PUNCT
eurjchem-228	106	13	b	b	NOUN
eurjchem-228	106	14	)	)	PUNCT
eurjchem-228	106	15	a	a	DET
eurjchem-228	106	16	mixture	mixture	NOUN
eurjchem-228	106	17	of	of	ADP
eurjchem-228	106	18	compound	compound	NOUN
eurjchem-228	106	19	2a	2a	NUM
eurjchem-228	106	20	(	(	PUNCT
eurjchem-228	106	21	0.02	0.02	NUM
eurjchem-228	106	22	mol	mol	NOUN
eurjchem-228	106	23	)	)	PUNCT
eurjchem-228	106	24	,	,	PUNCT
eurjchem-228	106	25	2b	2b	NUM
eurjchem-228	106	26	or	or	CCONJ
eurjchem-228	106	27	2c	2c	NUM
eurjchem-228	106	28	(	(	PUNCT
eurjchem-228	106	29	0.1	0.1	NUM
eurjchem-228	106	30	mol	mol	NOUN
eurjchem-228	106	31	)	)	PUNCT
eurjchem-228	106	32	and	and	CCONJ
eurjchem-228	106	33	acetic	acetic	ADJ
eurjchem-228	106	34	acid	acid	NOUN
eurjchem-228	106	35	(	(	PUNCT
eurjchem-228	106	36	0.5	0.5	NUM
eurjchem-228	106	37	ml	ml	NOUN
eurjchem-228	106	38	)	)	PUNCT
eurjchem-228	106	39	was	be	AUX
eurjchem-228	106	40	irradiated	irradiate	VERB
eurjchem-228	106	41	by	by	ADP
eurjchem-228	106	42	focused	focused	ADJ
eurjchem-228	106	43	microwave	microwave	NOUN
eurjchem-228	106	44	at	at	ADP
eurjchem-228	106	45	140	140	NUM
eurjchem-228	106	46	°	°	ADP
eurjchem-228	106	47	c	c	NOUN
eurjchem-228	106	48	for	for	ADP
eurjchem-228	106	49	30	30	NUM
eurjchem-228	106	50	min	min	NOUN
eurjchem-228	106	51	.	.	PUNCT
eurjchem-228	107	1	the	the	DET
eurjchem-228	107	2	solid	solid	ADJ
eurjchem-228	107	3	product	product	NOUN
eurjchem-228	107	4	,	,	PUNCT
eurjchem-228	107	5	so	so	ADV
eurjchem-228	107	6	formed	form	VERB
eurjchem-228	107	7	,	,	PUNCT
eurjchem-228	107	8	was	be	AUX
eurjchem-228	107	9	collected	collect	VERB
eurjchem-228	107	10	and	and	CCONJ
eurjchem-228	107	11	crystallized	crystallize	VERB
eurjchem-228	107	12	from	from	ADP
eurjchem-228	107	13	dioxane	dioxane	NOUN
eurjchem-228	107	14	to	to	PART
eurjchem-228	107	15	afford	afford	VERB
eurjchem-228	107	16	compounds	compound	NOUN
eurjchem-228	107	17	8a	8a	NUM
eurjchem-228	107	18	,	,	PUNCT
eurjchem-228	107	19	b.	b.	NOUN
eurjchem-228	107	20	2‐2‐[3‐[2‐(1,3‐dioxo‐2,3‐dihydro‐1h‐2‐isoindolyl)acetyl]‐5‐	2‐2‐[3‐[2‐(1,3‐dioxo‐2,3‐dihydro‐1h‐2‐isoindolyl)acetyl]‐5‐	NUM
eurjchem-228	107	21	(	(	PUNCT
eurjchem-228	107	22	1h‐2‐pyrrolylcarbony)phenyl]‐2‐oxoethyl‐1,3‐isoindolinedione	1h‐2‐pyrrolylcarbony)phenyl]‐2‐oxoethyl‐1,3‐isoindolinedione	NUM
eurjchem-228	107	23	,	,	PUNCT
eurjchem-228	107	24	8a	8a	NUM
eurjchem-228	107	25	:	:	PUNCT
eurjchem-228	107	26	buff	buff	PROPN
eurjchem-228	107	27	powder	powder	NOUN
eurjchem-228	107	28	.	.	PUNCT
eurjchem-228	108	1	yield	yield	NOUN
eurjchem-228	108	2	:	:	PUNCT
eurjchem-228	108	3	52	52	NUM
eurjchem-228	108	4	%	%	NOUN
eurjchem-228	108	5	.	.	PUNCT
eurjchem-228	109	1	m.p	m.p	PROPN
eurjchem-228	109	2	.	.	PROPN
eurjchem-228	109	3	:	:	PUNCT
eurjchem-228	110	1	252‐253	252‐253	NUM
eurjchem-228	110	2	°	°	ADP
eurjchem-228	110	3	c	c	NOUN
eurjchem-228	110	4	.	.	PUNCT
eurjchem-228	111	1	ft‐ir	ft‐ir	NOUN
eurjchem-228	111	2	(	(	PUNCT
eurjchem-228	111	3	kbr	kbr	PROPN
eurjchem-228	111	4	,	,	PUNCT
eurjchem-228	111	5	cm‐	cm‐	NOUN
eurjchem-228	111	6	1	1	NUM
eurjchem-228	111	7	):	):	PUNCT
eurjchem-228	111	8	3343	3343	NUM
eurjchem-228	111	9	(	(	PUNCT
eurjchem-228	111	10	nh	nh	NOUN
eurjchem-228	111	11	)	)	PUNCT
eurjchem-228	111	12	,	,	PUNCT
eurjchem-228	111	13	1717	1717	NUM
eurjchem-228	111	14	(	(	PUNCT
eurjchem-228	111	15	co	co	NOUN
eurjchem-228	111	16	)	)	PUNCT
eurjchem-228	111	17	.	.	PUNCT
eurjchem-228	112	1	1h	1h	NUM
eurjchem-228	112	2	nmr	nmr	NOUN
eurjchem-228	112	3	(	(	PUNCT
eurjchem-228	112	4	400	400	NUM
eurjchem-228	112	5	mhz	mhz	NOUN
eurjchem-228	112	6	,	,	PUNCT
eurjchem-228	112	7	dmso‐d6	dmso‐d6	NUM
eurjchem-228	112	8	):	):	PUNCT
eurjchem-228	112	9	5.54	5.54	NUM
eurjchem-228	112	10	(	(	PUNCT
eurjchem-228	112	11	d	d	PROPN
eurjchem-228	112	12	,	,	PUNCT
eurjchem-228	112	13	4h	4h	NUM
eurjchem-228	112	14	,	,	PUNCT
eurjchem-228	112	15	j=12.4	j=12.4	PROPN
eurjchem-228	112	16	hz	hz	VERB
eurjchem-228	112	17	,	,	PUNCT
eurjchem-228	112	18	2nch2	2nch2	NUM
eurjchem-228	112	19	)	)	PUNCT
eurjchem-228	112	20	,	,	PUNCT
eurjchem-228	112	21	6.23‐6.33	6.23‐6.33	NUM
eurjchem-228	112	22	(	(	PUNCT
eurjchem-228	112	23	m	m	PROPN
eurjchem-228	112	24	,	,	PUNCT
eurjchem-228	112	25	1h	1h	NUM
eurjchem-228	112	26	,	,	PUNCT
eurjchem-228	112	27	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	112	28	)	)	PUNCT
eurjchem-228	112	29	,	,	PUNCT
eurjchem-228	112	30	6.93‐	6.93‐	NUM
eurjchem-228	112	31	6.96	6.96	NUM
eurjchem-228	112	32	(	(	PUNCT
eurjchem-228	112	33	m	m	PROPN
eurjchem-228	112	34	,	,	PUNCT
eurjchem-228	112	35	1h	1h	NUM
eurjchem-228	112	36	,	,	PUNCT
eurjchem-228	112	37	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	112	38	)	)	PUNCT
eurjchem-228	112	39	,	,	PUNCT
eurjchem-228	112	40	7.31‐7.33	7.31‐7.33	NUM
eurjchem-228	112	41	(	(	PUNCT
eurjchem-228	112	42	m	m	PROPN
eurjchem-228	112	43	,	,	PUNCT
eurjchem-228	112	44	1h	1h	NUM
eurjchem-228	112	45	,	,	PUNCT
eurjchem-228	112	46	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	112	47	)	)	PUNCT
eurjchem-228	112	48	,	,	PUNCT
eurjchem-228	112	49	7.91‐	7.91‐	NUM
eurjchem-228	112	50	7.95	7.95	NUM
eurjchem-228	112	51	(	(	PUNCT
eurjchem-228	112	52	m	m	PROPN
eurjchem-228	112	53	,	,	PUNCT
eurjchem-228	112	54	4h	4h	NUM
eurjchem-228	112	55	,	,	PUNCT
eurjchem-228	112	56	ar‐h	ar‐h	PROPN
eurjchem-228	112	57	)	)	PUNCT
eurjchem-228	112	58	,	,	PUNCT
eurjchem-228	112	59	7.98‐8.00	7.98‐8.00	NUM
eurjchem-228	112	60	(	(	PUNCT
eurjchem-228	112	61	m	m	PROPN
eurjchem-228	112	62	,	,	PUNCT
eurjchem-228	112	63	4h	4h	NOUN
eurjchem-228	112	64	,	,	PUNCT
eurjchem-228	112	65	ar‐h	ar‐h	PROPN
eurjchem-228	112	66	)	)	PUNCT
eurjchem-228	112	67	,	,	PUNCT
eurjchem-228	112	68	8.62	8.62	NUM
eurjchem-228	112	69	(	(	PUNCT
eurjchem-228	112	70	d	d	PROPN
eurjchem-228	112	71	,	,	PUNCT
eurjchem-228	112	72	1h	1h	NUM
eurjchem-228	112	73	,	,	PUNCT
eurjchem-228	112	74	j=1.2	j=1.2	NOUN
eurjchem-228	112	75	hz	hz	NOUN
eurjchem-228	112	76	,	,	PUNCT
eurjchem-228	112	77	ch	ch	NOUN
eurjchem-228	112	78	)	)	PUNCT
eurjchem-228	112	79	,	,	PUNCT
eurjchem-228	112	80	8.98	8.98	NUM
eurjchem-228	112	81	(	(	PUNCT
eurjchem-228	112	82	s	s	PROPN
eurjchem-228	112	83	,	,	PUNCT
eurjchem-228	112	84	1h	1h	NUM
eurjchem-228	112	85	,	,	PUNCT
eurjchem-228	112	86	ch	ch	NOUN
eurjchem-228	112	87	)	)	PUNCT
eurjchem-228	112	88	,	,	PUNCT
eurjchem-228	112	89	12.29	12.29	NUM
eurjchem-228	112	90	(	(	PUNCT
eurjchem-228	112	91	s	s	PROPN
eurjchem-228	112	92	,	,	PUNCT
eurjchem-228	112	93	1h	1h	NUM
eurjchem-228	112	94	,	,	PUNCT
eurjchem-228	112	95	nh	nh	PROPN
eurjchem-228	112	96	)	)	PUNCT
eurjchem-228	112	97	.	.	PUNCT
eurjchem-228	113	1	ms	ms	NOUN
eurjchem-228	113	2	(	(	PUNCT
eurjchem-228	113	3	ei	ei	PROPN
eurjchem-228	113	4	,	,	PUNCT
eurjchem-228	113	5	m	m	PROPN
eurjchem-228	113	6	/	/	SYM
eurjchem-228	113	7	z	z	NOUN
eurjchem-228	113	8	,	,	PUNCT
eurjchem-228	113	9	%	%	INTJ
eurjchem-228	113	10	):	):	PUNCT
eurjchem-228	113	11	545	545	NUM
eurjchem-228	114	1	[	[	X
eurjchem-228	114	2	m+	m+	NUM
eurjchem-228	114	3	,	,	PUNCT
eurjchem-228	114	4	18	18	NUM
eurjchem-228	114	5	%	%	NOUN
eurjchem-228	114	6	]	]	PUNCT
eurjchem-228	114	7	.	.	PUNCT
eurjchem-228	115	1	anal	anal	PROPN
eurjchem-228	115	2	.	.	PUNCT
eurjchem-228	115	3	calcd	calcd	NOUN
eurjchem-228	115	4	.	.	PUNCT
eurjchem-228	116	1	for	for	ADP
eurjchem-228	116	2	c31h19n3o7	c31h19n3o7	NOUN
eurjchem-228	116	3	:	:	PUNCT
eurjchem-228	116	4	c	c	X
eurjchem-228	116	5	,	,	PUNCT
eurjchem-228	116	6	68.26	68.26	NUM
eurjchem-228	116	7	;	;	PUNCT
eurjchem-228	116	8	h	h	NOUN
eurjchem-228	116	9	,	,	PUNCT
eurjchem-228	116	10	3.51	3.51	NUM
eurjchem-228	116	11	;	;	PUNCT
eurjchem-228	116	12	n	n	CCONJ
eurjchem-228	116	13	,	,	PUNCT
eurjchem-228	116	14	7.70	7.70	NUM
eurjchem-228	116	15	.	.	PUNCT
eurjchem-228	116	16	found	find	VERB
eurjchem-228	116	17	:	:	PUNCT
eurjchem-228	117	1	68.37	68.37	NUM
eurjchem-228	117	2	;	;	PUNCT
eurjchem-228	117	3	h	h	X
eurjchem-228	117	4	,	,	PUNCT
eurjchem-228	117	5	3.91	3.91	NUM
eurjchem-228	117	6	;	;	PUNCT
eurjchem-228	117	7	n	n	CCONJ
eurjchem-228	117	8	,	,	PUNCT
eurjchem-228	117	9	7.74	7.74	NUM
eurjchem-228	117	10	.	.	PUNCT
eurjchem-228	118	1	2‐(2‐3‐benzoyl‐5‐[2‐(1,3‐dioxo‐2,3‐dihydro‐1h‐2‐isoindolyl	2‐(2‐3‐benzoyl‐5‐[2‐(1,3‐dioxo‐2,3‐dihydro‐1h‐2‐isoindolyl	NUM
eurjchem-228	118	2	)	)	PUNCT
eurjchem-228	118	3	acetyl]phenyl‐2‐oxoethyl)‐1,3‐isoindolinedione	acetyl]phenyl‐2‐oxoethyl)‐1,3‐isoindolinedione	NOUN
eurjchem-228	118	4	,	,	PUNCT
eurjchem-228	118	5	8b	8b	NUM
eurjchem-228	118	6	:	:	PUNCT
eurjchem-228	118	7	brown	brown	ADJ
eurjchem-228	118	8	powder	powder	NOUN
eurjchem-228	118	9	.	.	PUNCT
eurjchem-228	119	1	yield	yield	NOUN
eurjchem-228	119	2	:	:	PUNCT
eurjchem-228	119	3	68	68	NUM
eurjchem-228	119	4	%	%	NOUN
eurjchem-228	119	5	.	.	PUNCT
eurjchem-228	120	1	m.p	m.p	PROPN
eurjchem-228	120	2	.	.	PROPN
eurjchem-228	120	3	:	:	PUNCT
eurjchem-228	121	1	194‐496	194‐496	NUM
eurjchem-228	121	2	°	°	SYM
eurjchem-228	121	3	c	c	X
eurjchem-228	121	4	.	.	PUNCT
eurjchem-228	122	1	ft‐ir	ft‐ir	NOUN
eurjchem-228	122	2	(	(	PUNCT
eurjchem-228	122	3	kbr	kbr	PROPN
eurjchem-228	122	4	,	,	PUNCT
eurjchem-228	122	5	cm‐1	cm‐1	PROPN
eurjchem-228	122	6	):	):	PUNCT
eurjchem-228	122	7	1718	1718	NUM
eurjchem-228	122	8	(	(	PUNCT
eurjchem-228	122	9	co	co	NOUN
eurjchem-228	122	10	)	)	PUNCT
eurjchem-228	122	11	.	.	PUNCT
eurjchem-228	123	1	1h	1h	NUM
eurjchem-228	123	2	nmr	nmr	NOUN
eurjchem-228	123	3	(	(	PUNCT
eurjchem-228	123	4	400	400	NUM
eurjchem-228	123	5	mhz	mhz	NOUN
eurjchem-228	123	6	,	,	PUNCT
eurjchem-228	123	7	dmso‐d6	dmso‐d6	NUM
eurjchem-228	123	8	):	):	PUNCT
eurjchem-228	123	9	5.55	5.55	NUM
eurjchem-228	123	10	(	(	PUNCT
eurjchem-228	123	11	d	d	PROPN
eurjchem-228	123	12	,	,	PUNCT
eurjchem-228	123	13	4h	4h	NUM
eurjchem-228	123	14	,	,	PUNCT
eurjchem-228	123	15	j=7.6	j=7.6	PROPN
eurjchem-228	123	16	hz	hz	VERB
eurjchem-228	123	17	,	,	PUNCT
eurjchem-228	123	18	2nch2	2nch2	NUM
eurjchem-228	123	19	)	)	PUNCT
eurjchem-228	123	20	,	,	PUNCT
eurjchem-228	123	21	7.30‐732	7.30‐732	NUM
eurjchem-228	123	22	(	(	PUNCT
eurjchem-228	123	23	m	m	PROPN
eurjchem-228	123	24	,	,	PUNCT
eurjchem-228	123	25	3h	3h	NUM
eurjchem-228	123	26	,	,	PUNCT
eurjchem-228	123	27	ar‐h	ar‐h	NOUN
eurjchem-228	123	28	)	)	PUNCT
eurjchem-228	123	29	,	,	PUNCT
eurjchem-228	123	30	7.56‐7.59	7.56‐7.59	NUM
eurjchem-228	123	31	(	(	PUNCT
eurjchem-228	123	32	m	m	PROPN
eurjchem-228	123	33	,	,	PUNCT
eurjchem-228	123	34	2h	2h	NUM
eurjchem-228	123	35	,	,	PUNCT
eurjchem-228	123	36	ar‐h	ar‐h	NOUN
eurjchem-228	123	37	)	)	PUNCT
eurjchem-228	123	38	,	,	PUNCT
eurjchem-228	123	39	7.83‐	7.83‐	NUM
eurjchem-228	123	40	7.87	7.87	NUM
eurjchem-228	123	41	(	(	PUNCT
eurjchem-228	123	42	m	m	PROPN
eurjchem-228	123	43	,	,	PUNCT
eurjchem-228	123	44	4h	4h	NUM
eurjchem-228	123	45	,	,	PUNCT
eurjchem-228	123	46	ar‐h	ar‐h	PROPN
eurjchem-228	123	47	)	)	PUNCT
eurjchem-228	123	48	,	,	PUNCT
eurjchem-228	123	49	7.93‐7.98	7.93‐7.98	NUM
eurjchem-228	123	50	(	(	PUNCT
eurjchem-228	123	51	m	m	PROPN
eurjchem-228	123	52	,	,	PUNCT
eurjchem-228	123	53	4h	4h	NOUN
eurjchem-228	123	54	,	,	PUNCT
eurjchem-228	123	55	ar‐h	ar‐h	PROPN
eurjchem-228	123	56	)	)	PUNCT
eurjchem-228	123	57	,	,	PUNCT
eurjchem-228	123	58	8.57	8.57	NUM
eurjchem-228	123	59	(	(	PUNCT
eurjchem-228	123	60	s	s	PROPN
eurjchem-228	123	61	,	,	PUNCT
eurjchem-228	123	62	1h	1h	NUM
eurjchem-228	123	63	,	,	PUNCT
eurjchem-228	123	64	ch	ch	NOUN
eurjchem-228	123	65	)	)	PUNCT
eurjchem-228	123	66	,	,	PUNCT
eurjchem-228	123	67	8.98	8.98	NUM
eurjchem-228	123	68	(	(	PUNCT
eurjchem-228	123	69	s	s	PROPN
eurjchem-228	123	70	,	,	PUNCT
eurjchem-228	123	71	1h	1h	NUM
eurjchem-228	123	72	,	,	PUNCT
eurjchem-228	123	73	ch	ch	NOUN
eurjchem-228	123	74	)	)	PUNCT
eurjchem-228	123	75	.	.	PUNCT
eurjchem-228	124	1	ms	ms	NOUN
eurjchem-228	124	2	(	(	PUNCT
eurjchem-228	124	3	ei	ei	PROPN
eurjchem-228	124	4	,	,	PUNCT
eurjchem-228	124	5	m	m	PROPN
eurjchem-228	124	6	/	/	SYM
eurjchem-228	124	7	z	z	NOUN
eurjchem-228	124	8	,	,	PUNCT
eurjchem-228	124	9	%	%	INTJ
eurjchem-228	124	10	):	):	PUNCT
eurjchem-228	124	11	556	556	NUM
eurjchem-228	124	12	[	[	X
eurjchem-228	124	13	m+	m+	NUM
eurjchem-228	124	14	,	,	PUNCT
eurjchem-228	124	15	32	32	NUM
eurjchem-228	124	16	%	%	NOUN
eurjchem-228	124	17	]	]	PUNCT
eurjchem-228	124	18	.	.	PUNCT
eurjchem-228	125	1	anal	anal	ADJ
eurjchem-228	125	2	.	.	PUNCT
eurjchem-228	125	3	calcd	calcd	NOUN
eurjchem-228	125	4	.	.	PUNCT
eurjchem-228	126	1	for	for	ADP
eurjchem-228	126	2	c33h20n2o7	c33h20n2o7	NOUN
eurjchem-228	126	3	:	:	PUNCT
eurjchem-228	126	4	c	c	X
eurjchem-228	126	5	,	,	PUNCT
eurjchem-228	126	6	71.22	71.22	NUM
eurjchem-228	126	7	;	;	PUNCT
eurjchem-228	126	8	h	h	NOUN
eurjchem-228	126	9	,	,	PUNCT
eurjchem-228	126	10	3.62	3.62	NUM
eurjchem-228	126	11	;	;	PUNCT
eurjchem-228	126	12	n	n	CCONJ
eurjchem-228	126	13	,	,	PUNCT
eurjchem-228	126	14	5.03	5.03	NUM
eurjchem-228	126	15	.	.	PUNCT
eurjchem-228	126	16	found	find	VERB
eurjchem-228	126	17	:	:	PUNCT
eurjchem-228	127	1	c	c	X
eurjchem-228	127	2	,	,	PUNCT
eurjchem-228	127	3	70.94	70.94	NUM
eurjchem-228	127	4	;	;	PUNCT
eurjchem-228	127	5	h	h	NOUN
eurjchem-228	127	6	,	,	PUNCT
eurjchem-228	127	7	3.96	3.96	NUM
eurjchem-228	127	8	;	;	PUNCT
eurjchem-228	127	9	n	n	CCONJ
eurjchem-228	127	10	,	,	PUNCT
eurjchem-228	127	11	5.72	5.72	NUM
eurjchem-228	127	12	.	.	NOUN
eurjchem-228	127	13	2.5	2.5	NUM
eurjchem-228	127	14	.	.	PUNCT
eurjchem-228	128	1	general	general	ADJ
eurjchem-228	128	2	procedure	procedure	NOUN
eurjchem-228	128	3	for	for	ADP
eurjchem-228	128	4	the	the	DET
eurjchem-228	128	5	synthesis	synthesis	NOUN
eurjchem-228	128	6	of	of	ADP
eurjchem-228	128	7	compounds	compound	NOUN
eurjchem-228	128	8	(	(	PUNCT
eurjchem-228	128	9	9a‐c	9a‐c	NOUN
eurjchem-228	128	10	)	)	PUNCT
eurjchem-228	128	11	a	a	DET
eurjchem-228	128	12	mixture	mixture	NOUN
eurjchem-228	128	13	of	of	ADP
eurjchem-228	128	14	compounds	compound	NOUN
eurjchem-228	128	15	2a‐c	2a‐c	NOUN
eurjchem-228	128	16	(	(	PUNCT
eurjchem-228	128	17	0.01	0.01	NUM
eurjchem-228	128	18	mol	mol	NOUN
eurjchem-228	128	19	)	)	PUNCT
eurjchem-228	128	20	,	,	PUNCT
eurjchem-228	128	21	etoh	etoh	PROPN
eurjchem-228	128	22	(	(	PUNCT
eurjchem-228	128	23	1	1	NUM
eurjchem-228	128	24	ml	ml	NOUN
eurjchem-228	128	25	)	)	PUNCT
eurjchem-228	128	26	and	and	CCONJ
eurjchem-228	128	27	aniline	aniline	NOUN
eurjchem-228	128	28	(	(	PUNCT
eurjchem-228	128	29	0.93	0.93	NUM
eurjchem-228	128	30	g	g	NOUN
eurjchem-228	128	31	,	,	PUNCT
eurjchem-228	128	32	0.01	0.01	NUM
eurjchem-228	128	33	mol	mol	NOUN
eurjchem-228	128	34	)	)	PUNCT
eurjchem-228	128	35	were	be	AUX
eurjchem-228	128	36	irradiated	irradiate	VERB
eurjchem-228	128	37	by	by	ADP
eurjchem-228	128	38	focused	focused	ADJ
eurjchem-228	128	39	microwave	microwave	NOUN
eurjchem-228	128	40	at	at	ADP
eurjchem-228	128	41	140	140	NUM
eurjchem-228	128	42	°	°	ADP
eurjchem-228	128	43	c	c	NOUN
eurjchem-228	128	44	for	for	ADP
eurjchem-228	128	45	5	5	NUM
eurjchem-228	128	46	min	min	NOUN
eurjchem-228	128	47	.	.	PUNCT
eurjchem-228	129	1	the	the	DET
eurjchem-228	129	2	reaction	reaction	NOUN
eurjchem-228	129	3	mixture	mixture	NOUN
eurjchem-228	129	4	was	be	AUX
eurjchem-228	129	5	poured	pour	VERB
eurjchem-228	129	6	into	into	ADP
eurjchem-228	129	7	cold	cold	ADJ
eurjchem-228	129	8	water	water	NOUN
eurjchem-228	129	9	,	,	PUNCT
eurjchem-228	129	10	filtered	filter	VERB
eurjchem-228	129	11	and	and	CCONJ
eurjchem-228	129	12	crystallized	crystallize	VERB
eurjchem-228	129	13	from	from	ADP
eurjchem-228	129	14	ethanol	ethanol	NOUN
eurjchem-228	129	15	to	to	PART
eurjchem-228	129	16	afford	afford	VERB
eurjchem-228	129	17	compounds	compound	NOUN
eurjchem-228	129	18	9a‐c	9a‐c	PROPN
eurjchem-228	129	19	.	.	PUNCT
eurjchem-228	130	1	2‐(2‐oxo‐4‐phenylamino‐but‐3‐enyl)isoindole‐1,3‐dione	2‐(2‐oxo‐4‐phenylamino‐but‐3‐enyl)isoindole‐1,3‐dione	NUM
eurjchem-228	130	2	,	,	PUNCT
eurjchem-228	130	3	9a	9a	NUM
eurjchem-228	130	4	:	:	PUNCT
eurjchem-228	130	5	yellow‐orange	yellow‐orange	NOUN
eurjchem-228	130	6	crystals	crystal	NOUN
eurjchem-228	130	7	.	.	PUNCT
eurjchem-228	131	1	yield	yield	NOUN
eurjchem-228	131	2	:	:	PUNCT
eurjchem-228	131	3	88	88	NUM
eurjchem-228	131	4	%	%	NOUN
eurjchem-228	131	5	.	.	PUNCT
eurjchem-228	132	1	m.p	m.p	PROPN
eurjchem-228	132	2	.	.	PROPN
eurjchem-228	132	3	:	:	PUNCT
eurjchem-228	133	1	167‐169	167‐169	NUM
eurjchem-228	133	2	°	°	SYM
eurjchem-228	133	3	c	c	PROPN
eurjchem-228	133	4	.	.	PUNCT
eurjchem-228	134	1	ft‐ir	ft‐ir	NOUN
eurjchem-228	134	2	(	(	PUNCT
eurjchem-228	134	3	kbr	kbr	PROPN
eurjchem-228	134	4	,	,	PUNCT
eurjchem-228	134	5	cm‐1	cm‐1	PROPN
eurjchem-228	134	6	):	):	PUNCT
eurjchem-228	134	7	3457	3457	NUM
eurjchem-228	134	8	(	(	PUNCT
eurjchem-228	134	9	nh	nh	NOUN
eurjchem-228	134	10	)	)	PUNCT
eurjchem-228	134	11	,	,	PUNCT
eurjchem-228	134	12	1773	1773	NUM
eurjchem-228	134	13	,	,	PUNCT
eurjchem-228	134	14	1706	1706	NUM
eurjchem-228	134	15	,	,	PUNCT
eurjchem-228	134	16	1640	1640	NUM
eurjchem-228	134	17	(	(	PUNCT
eurjchem-228	134	18	co	co	NOUN
eurjchem-228	134	19	)	)	PUNCT
eurjchem-228	134	20	.	.	PUNCT
eurjchem-228	135	1	1h	1h	NUM
eurjchem-228	135	2	nmr	nmr	NOUN
eurjchem-228	135	3	(	(	PUNCT
eurjchem-228	135	4	400	400	NUM
eurjchem-228	135	5	mhz	mhz	NOUN
eurjchem-228	135	6	,	,	PUNCT
eurjchem-228	135	7	dmso‐d6	dmso‐d6	NUM
eurjchem-228	135	8	):	):	PUNCT
eurjchem-228	135	9	4.50	4.50	NUM
eurjchem-228	135	10	(	(	PUNCT
eurjchem-228	135	11	s	s	PROPN
eurjchem-228	135	12	,	,	PUNCT
eurjchem-228	135	13	2h	2h	NUM
eurjchem-228	135	14	,	,	PUNCT
eurjchem-228	135	15	nch2	nch2	PROPN
eurjchem-228	135	16	)	)	PUNCT
eurjchem-228	135	17	,	,	PUNCT
eurjchem-228	135	18	5.45	5.45	NUM
eurjchem-228	135	19	(	(	PUNCT
eurjchem-228	135	20	d	d	PROPN
eurjchem-228	135	21	,	,	PUNCT
eurjchem-228	135	22	1h	1h	NUM
eurjchem-228	135	23	,	,	PUNCT
eurjchem-228	135	24	j=8.0	j=8.0	PROPN
eurjchem-228	135	25	hz	hz	PROPN
eurjchem-228	135	26	,	,	PUNCT
eurjchem-228	135	27	ch	ch	NOUN
eurjchem-228	135	28	)	)	PUNCT
eurjchem-228	135	29	,	,	PUNCT
eurjchem-228	135	30	7.03	7.03	NUM
eurjchem-228	135	31	(	(	PUNCT
eurjchem-228	135	32	t	t	PROPN
eurjchem-228	135	33	,	,	PUNCT
eurjchem-228	135	34	1h	1h	NUM
eurjchem-228	135	35	,	,	PUNCT
eurjchem-228	135	36	j=7.2	j=7.2	NOUN
eurjchem-228	135	37	hz	hz	VERB
eurjchem-228	135	38	,	,	PUNCT
eurjchem-228	135	39	phenyl‐h	phenyl‐h	NOUN
eurjchem-228	135	40	)	)	PUNCT
eurjchem-228	135	41	,	,	PUNCT
eurjchem-228	135	42	7.25	7.25	NUM
eurjchem-228	135	43	(	(	PUNCT
eurjchem-228	135	44	d	d	PROPN
eurjchem-228	135	45	,	,	PUNCT
eurjchem-228	135	46	2h	2h	NUM
eurjchem-228	135	47	,	,	PUNCT
eurjchem-228	136	1	j=8.0	j=8.0	PROPN
eurjchem-228	136	2	hz	hz	PROPN
eurjchem-228	136	3	,	,	PUNCT
eurjchem-228	136	4	phenyl‐h	phenyl‐h	PROPN
eurjchem-228	136	5	)	)	PUNCT
eurjchem-228	136	6	,	,	PUNCT
eurjchem-228	136	7	7.30	7.30	NUM
eurjchem-228	136	8	(	(	PUNCT
eurjchem-228	136	9	t	t	PROPN
eurjchem-228	136	10	,	,	PUNCT
eurjchem-228	136	11	2h	2h	NUM
eurjchem-228	136	12	,	,	PUNCT
eurjchem-228	136	13	j=7.2	j=7.2	NOUN
eurjchem-228	136	14	hz	hz	VERB
eurjchem-228	136	15	,	,	PUNCT
eurjchem-228	136	16	phenyl‐h	phenyl‐h	NOUN
eurjchem-228	136	17	)	)	PUNCT
eurjchem-228	136	18	,	,	PUNCT
eurjchem-228	136	19	7.77	7.77	NUM
eurjchem-228	136	20	(	(	PUNCT
eurjchem-228	136	21	dd	dd	PROPN
eurjchem-228	136	22	,	,	PUNCT
eurjchem-228	136	23	1h	1h	NUM
eurjchem-228	136	24	,	,	PUNCT
eurjchem-228	136	25	j=8.0	j=8.0	PROPN
eurjchem-228	136	26	hz	hz	PROPN
eurjchem-228	136	27	,	,	PUNCT
eurjchem-228	136	28	j=8.0	j=8.0	PROPN
eurjchem-228	136	29	hz	hz	PROPN
eurjchem-228	136	30	ch	ch	PROPN
eurjchem-228	136	31	)	)	PUNCT
eurjchem-228	136	32	,	,	PUNCT
eurjchem-228	137	1	7.87‐7.90	7.87‐7.90	NUM
eurjchem-228	137	2	(	(	PUNCT
eurjchem-228	137	3	m	m	PROPN
eurjchem-228	137	4	,	,	PUNCT
eurjchem-228	137	5	2h	2h	NUM
eurjchem-228	137	6	,	,	PUNCT
eurjchem-228	137	7	phthalimidyl‐h	phthalimidyl‐h	NOUN
eurjchem-228	137	8	)	)	PUNCT
eurjchem-228	137	9	,	,	PUNCT
eurjchem-228	137	10	7.91‐7.95	7.91‐7.95	NUM
eurjchem-228	137	11	(	(	PUNCT
eurjchem-228	137	12	m	m	PROPN
eurjchem-228	137	13	,	,	PUNCT
eurjchem-228	137	14	2h	2h	NUM
eurjchem-228	137	15	,	,	PUNCT
eurjchem-228	137	16	phthalimidyl‐h	phthalimidyl‐h	NOUN
eurjchem-228	137	17	)	)	PUNCT
eurjchem-228	137	18	,	,	PUNCT
eurjchem-228	137	19	11.15	11.15	NUM
eurjchem-228	137	20	(	(	PUNCT
eurjchem-228	137	21	d	d	PROPN
eurjchem-228	137	22	,	,	PUNCT
eurjchem-228	137	23	1h	1h	NUM
eurjchem-228	137	24	,	,	PUNCT
eurjchem-228	137	25	j=12.6	j=12.6	PROPN
eurjchem-228	137	26	hz	hz	PROPN
eurjchem-228	137	27	,	,	PUNCT
eurjchem-228	137	28	nh	nh	PROPN
eurjchem-228	137	29	)	)	PUNCT
eurjchem-228	137	30	.	.	PUNCT
eurjchem-228	138	1	13c	13c	NOUN
eurjchem-228	138	2	nmr	nmr	NOUN
eurjchem-228	138	3	(	(	PUNCT
eurjchem-228	138	4	dmso‐	dmso‐	PROPN
eurjchem-228	138	5	d6	d6	NOUN
eurjchem-228	138	6	,	,	PUNCT
eurjchem-228	138	7	100	100	NUM
eurjchem-228	138	8	mhz	mhz	NOUN
eurjchem-228	138	9	):	):	PUNCT
eurjchem-228	138	10	191.47	191.47	NUM
eurjchem-228	138	11	,	,	PUNCT
eurjchem-228	138	12	168.22	168.22	NUM
eurjchem-228	138	13	(	(	PUNCT
eurjchem-228	138	14	co	co	NOUN
eurjchem-228	138	15	)	)	PUNCT
eurjchem-228	138	16	,	,	PUNCT
eurjchem-228	138	17	145.75	145.75	NUM
eurjchem-228	138	18	,	,	PUNCT
eurjchem-228	138	19	140.38	140.38	NUM
eurjchem-228	138	20	,	,	PUNCT
eurjchem-228	138	21	135.16	135.16	NUM
eurjchem-228	138	22	,	,	PUNCT
eurjchem-228	138	23	132.14	132.14	NUM
eurjchem-228	138	24	,	,	PUNCT
eurjchem-228	138	25	130.06	130.06	NUM
eurjchem-228	138	26	,	,	PUNCT
eurjchem-228	138	27	123.96	123.96	NUM
eurjchem-228	138	28	,	,	PUNCT
eurjchem-228	138	29	123.69	123.69	NUM
eurjchem-228	138	30	,	,	PUNCT
eurjchem-228	138	31	116.66	116.66	NUM
eurjchem-228	138	32	,	,	PUNCT
eurjchem-228	138	33	93.58	93.58	NUM
eurjchem-228	138	34	,	,	PUNCT
eurjchem-228	138	35	45.79	45.79	NUM
eurjchem-228	138	36	(	(	PUNCT
eurjchem-228	138	37	nch2	nch2	PROPN
eurjchem-228	138	38	)	)	PUNCT
eurjchem-228	138	39	.	.	PUNCT
eurjchem-228	139	1	ms	ms	NOUN
eurjchem-228	139	2	(	(	PUNCT
eurjchem-228	139	3	ei	ei	PROPN
eurjchem-228	139	4	,	,	PUNCT
eurjchem-228	139	5	m	m	PROPN
eurjchem-228	139	6	/	/	SYM
eurjchem-228	139	7	z	z	NOUN
eurjchem-228	139	8	,	,	PUNCT
eurjchem-228	139	9	%	%	INTJ
eurjchem-228	139	10	):	):	PUNCT
eurjchem-228	139	11	306	306	NUM
eurjchem-228	140	1	[	[	X
eurjchem-228	140	2	m+	m+	NUM
eurjchem-228	140	3	,	,	PUNCT
eurjchem-228	140	4	20	20	NUM
eurjchem-228	140	5	%	%	NOUN
eurjchem-228	140	6	]	]	X
eurjchem-228	140	7	;	;	PUNCT
eurjchem-228	140	8	160	160	NUM
eurjchem-228	140	9	(	(	PUNCT
eurjchem-228	140	10	25	25	NUM
eurjchem-228	140	11	)	)	PUNCT
eurjchem-228	140	12	,	,	PUNCT
eurjchem-228	140	13	146	146	NUM
eurjchem-228	140	14	(	(	PUNCT
eurjchem-228	140	15	100	100	NUM
eurjchem-228	140	16	)	)	PUNCT
eurjchem-228	140	17	,	,	PUNCT
eurjchem-228	140	18	117	117	NUM
eurjchem-228	140	19	(	(	PUNCT
eurjchem-228	140	20	8)	8)	NUM
eurjchem-228	140	21	,	,	PUNCT
eurjchem-228	140	22	104	104	NUM
eurjchem-228	140	23	(	(	PUNCT
eurjchem-228	140	24	14	14	NUM
eurjchem-228	140	25	)	)	PUNCT
eurjchem-228	140	26	,	,	PUNCT
eurjchem-228	140	27	77	77	NUM
eurjchem-228	140	28	(	(	PUNCT
eurjchem-228	140	29	12	12	NUM
eurjchem-228	140	30	)	)	PUNCT
eurjchem-228	140	31	.	.	PUNCT
eurjchem-228	141	1	anal	anal	PROPN
eurjchem-228	141	2	.	.	PUNCT
eurjchem-228	141	3	calcd	calcd	NOUN
eurjchem-228	141	4	.	.	PUNCT
eurjchem-228	142	1	for	for	ADP
eurjchem-228	142	2	c18h14n2o3	c18h14n2o3	PROPN
eurjchem-228	142	3	:	:	PUNCT
eurjchem-228	142	4	c	c	X
eurjchem-228	142	5	,	,	PUNCT
eurjchem-228	142	6	70.58	70.58	NUM
eurjchem-228	142	7	;	;	PUNCT
eurjchem-228	142	8	h	h	NOUN
eurjchem-228	142	9	,	,	PUNCT
eurjchem-228	142	10	4.61	4.61	NUM
eurjchem-228	142	11	,	,	PUNCT
eurjchem-228	142	12	n	n	CCONJ
eurjchem-228	142	13	,	,	PUNCT
eurjchem-228	142	14	9.15	9.15	NUM
eurjchem-228	142	15	.	.	PUNCT
eurjchem-228	142	16	found	find	VERB
eurjchem-228	142	17	:	:	PUNCT
eurjchem-228	143	1	c	c	X
eurjchem-228	143	2	,	,	PUNCT
eurjchem-228	143	3	70.55	70.55	NUM
eurjchem-228	143	4	;	;	PUNCT
eurjchem-228	144	1	h	h	NOUN
eurjchem-228	144	2	,	,	PUNCT
eurjchem-228	144	3	4.61	4.61	NUM
eurjchem-228	144	4	,	,	PUNCT
eurjchem-228	144	5	n	n	CCONJ
eurjchem-228	144	6	,	,	PUNCT
eurjchem-228	144	7	9.27	9.27	NUM
eurjchem-228	144	8	.	.	PUNCT
eurjchem-228	145	1	3‐phenylamino‐1‐(1h‐pyrrol‐2‐yl)‐propenone	3‐phenylamino‐1‐(1h‐pyrrol‐2‐yl)‐propenone	NUM
eurjchem-228	145	2	,	,	PUNCT
eurjchem-228	145	3	9b	9b	NUM
eurjchem-228	145	4	:	:	PUNCT
eurjchem-228	145	5	golden‐	golden‐	VERB
eurjchem-228	145	6	yellow	yellow	ADJ
eurjchem-228	145	7	crystals	crystal	NOUN
eurjchem-228	145	8	.	.	PUNCT
eurjchem-228	146	1	yield	yield	NOUN
eurjchem-228	146	2	:	:	PUNCT
eurjchem-228	146	3	74	74	NUM
eurjchem-228	146	4	%	%	NOUN
eurjchem-228	146	5	.	.	PUNCT
eurjchem-228	147	1	m.p	m.p	PROPN
eurjchem-228	147	2	.	.	PROPN
eurjchem-228	147	3	:	:	PUNCT
eurjchem-228	148	1	217‐218	217‐218	NOUN
eurjchem-228	148	2	°	°	SYM
eurjchem-228	148	3	c	c	NOUN
eurjchem-228	148	4	.	.	PUNCT
eurjchem-228	149	1	ft‐ir	ft‐ir	NOUN
eurjchem-228	149	2	(	(	PUNCT
eurjchem-228	149	3	kbr	kbr	PROPN
eurjchem-228	149	4	,	,	PUNCT
eurjchem-228	149	5	cm‐1	cm‐1	PROPN
eurjchem-228	149	6	):	):	PUNCT
eurjchem-228	149	7	3262	3262	NUM
eurjchem-228	149	8	(	(	PUNCT
eurjchem-228	149	9	nh	nh	NOUN
eurjchem-228	149	10	)	)	PUNCT
eurjchem-228	149	11	,	,	PUNCT
eurjchem-228	149	12	1635	1635	NUM
eurjchem-228	149	13	(	(	PUNCT
eurjchem-228	149	14	co	co	NOUN
eurjchem-228	149	15	)	)	PUNCT
eurjchem-228	149	16	.	.	PUNCT
eurjchem-228	150	1	1h	1h	NUM
eurjchem-228	150	2	nmr	nmr	NOUN
eurjchem-228	150	3	(	(	PUNCT
eurjchem-228	150	4	400	400	NUM
eurjchem-228	150	5	mhz	mhz	NOUN
eurjchem-228	150	6	,	,	PUNCT
eurjchem-228	150	7	dmso‐d6	dmso‐d6	NUM
eurjchem-228	150	8	):	):	PUNCT
eurjchem-228	150	9	5.85	5.85	NUM
eurjchem-228	150	10	(	(	PUNCT
eurjchem-228	150	11	d,1h	d,1h	PROPN
eurjchem-228	150	12	,	,	PUNCT
eurjchem-228	150	13	j=8.0	j=8.0	PROPN
eurjchem-228	150	14	hz	hz	PROPN
eurjchem-228	150	15	,	,	PUNCT
eurjchem-228	150	16	ch	ch	NOUN
eurjchem-228	150	17	)	)	PUNCT
eurjchem-228	150	18	,	,	PUNCT
eurjchem-228	150	19	6.16‐6.18	6.16‐6.18	NUM
eurjchem-228	150	20	(	(	PUNCT
eurjchem-228	150	21	m	m	PROPN
eurjchem-228	150	22	,	,	PUNCT
eurjchem-228	150	23	1h	1h	NUM
eurjchem-228	150	24	,	,	PUNCT
eurjchem-228	150	25	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	150	26	)	)	PUNCT
eurjchem-228	150	27	,	,	PUNCT
eurjchem-228	150	28	6.88‐6.90	6.88‐6.90	NUM
eurjchem-228	150	29	(	(	PUNCT
eurjchem-228	150	30	m	m	PROPN
eurjchem-228	150	31	,	,	PUNCT
eurjchem-228	150	32	1h	1h	NUM
eurjchem-228	150	33	,	,	PUNCT
eurjchem-228	150	34	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	150	35	)	)	PUNCT
eurjchem-228	150	36	,	,	PUNCT
eurjchem-228	150	37	7.00‐7.04	7.00‐7.04	NUM
eurjchem-228	150	38	(	(	PUNCT
eurjchem-228	150	39	m	m	PROPN
eurjchem-228	150	40	,	,	PUNCT
eurjchem-228	150	41	1h	1h	NUM
eurjchem-228	150	42	,	,	PUNCT
eurjchem-228	150	43	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	150	44	)	)	PUNCT
eurjchem-228	150	45	,	,	PUNCT
eurjchem-228	150	46	7.21	7.21	NUM
eurjchem-228	150	47	(	(	PUNCT
eurjchem-228	150	48	d,2h	d,2h	PROPN
eurjchem-228	150	49	,	,	PUNCT
eurjchem-228	150	50	j=8.4	j=8.4	NOUN
eurjchem-228	150	51	hz	hz	NOUN
eurjchem-228	150	52	,	,	PUNCT
eurjchem-228	150	53	phenyl‐h	phenyl‐h	NOUN
eurjchem-228	150	54	)	)	PUNCT
eurjchem-228	150	55	,	,	PUNCT
eurjchem-228	150	56	7.32	7.32	NUM
eurjchem-228	150	57	(	(	PUNCT
eurjchem-228	150	58	t	t	PROPN
eurjchem-228	150	59	,	,	PUNCT
eurjchem-228	150	60	3h	3h	NUM
eurjchem-228	150	61	,	,	PUNCT
eurjchem-228	150	62	j=8.4	j=8.4	NOUN
eurjchem-228	150	63	hz	hz	NOUN
eurjchem-228	150	64	,	,	PUNCT
eurjchem-228	150	65	phenyl‐h	phenyl‐h	NOUN
eurjchem-228	150	66	)	)	PUNCT
eurjchem-228	150	67	,	,	PUNCT
eurjchem-228	150	68	7.69	7.69	NUM
eurjchem-228	150	69	(	(	PUNCT
eurjchem-228	150	70	dd	dd	PROPN
eurjchem-228	150	71	,	,	PUNCT
eurjchem-228	150	72	1h	1h	NUM
eurjchem-228	150	73	,	,	PUNCT
eurjchem-228	150	74	j=8.0	j=8.0	PROPN
eurjchem-228	150	75	hz	hz	PROPN
eurjchem-228	150	76	,	,	PUNCT
eurjchem-228	150	77	j=8.0	j=8.0	PROPN
eurjchem-228	150	78	hz	hz	PROPN
eurjchem-228	150	79	,	,	PUNCT
eurjchem-228	150	80	ch	ch	NOUN
eurjchem-228	150	81	)	)	PUNCT
eurjchem-228	150	82	,	,	PUNCT
eurjchem-228	150	83	11.63	11.63	NUM
eurjchem-228	150	84	(	(	PUNCT
eurjchem-228	150	85	s	s	PROPN
eurjchem-228	150	86	,	,	PUNCT
eurjchem-228	150	87	1h	1h	NUM
eurjchem-228	150	88	,	,	PUNCT
eurjchem-228	150	89	nh	nh	PROPN
eurjchem-228	150	90	)	)	PUNCT
eurjchem-228	150	91	,	,	PUNCT
eurjchem-228	150	92	11.71	11.71	NUM
eurjchem-228	150	93	(	(	PUNCT
eurjchem-228	150	94	s	s	PROPN
eurjchem-228	150	95	,	,	PUNCT
eurjchem-228	150	96	1h	1h	NUM
eurjchem-228	150	97	,	,	PUNCT
eurjchem-228	150	98	nh	nh	PROPN
eurjchem-228	150	99	)	)	PUNCT
eurjchem-228	150	100	.	.	PUNCT
eurjchem-228	151	1	ms	ms	NOUN
eurjchem-228	151	2	(	(	PUNCT
eurjchem-228	151	3	ei	ei	PROPN
eurjchem-228	151	4	,	,	PUNCT
eurjchem-228	151	5	m	m	PROPN
eurjchem-228	151	6	/	/	SYM
eurjchem-228	151	7	z	z	NOUN
eurjchem-228	151	8	,	,	PUNCT
eurjchem-228	151	9	%	%	INTJ
eurjchem-228	151	10	):	):	PUNCT
eurjchem-228	151	11	212	212	NUM
eurjchem-228	151	12	[	[	X
eurjchem-228	151	13	m+	m+	NUM
eurjchem-228	151	14	,	,	PUNCT
eurjchem-228	151	15	100	100	NUM
eurjchem-228	151	16	%	%	NOUN
eurjchem-228	151	17	]	]	PUNCT
eurjchem-228	151	18	.	.	PUNCT
eurjchem-228	152	1	anal	anal	ADJ
eurjchem-228	152	2	.	.	PUNCT
eurjchem-228	152	3	calcd	calcd	NOUN
eurjchem-228	152	4	.	.	PUNCT
eurjchem-228	153	1	for	for	ADP
eurjchem-228	153	2	c13h12n2o	c13h12n2o	NOUN
eurjchem-228	153	3	:	:	PUNCT
eurjchem-228	153	4	c	c	X
eurjchem-228	153	5	,	,	PUNCT
eurjchem-228	153	6	73.56	73.56	NUM
eurjchem-228	153	7	;	;	PUNCT
eurjchem-228	153	8	h	h	NOUN
eurjchem-228	153	9	,	,	PUNCT
eurjchem-228	153	10	5.70	5.70	NUM
eurjchem-228	153	11	;	;	PUNCT
eurjchem-228	153	12	n	n	CCONJ
eurjchem-228	153	13	,	,	PUNCT
eurjchem-228	153	14	13.20	13.20	NUM
eurjchem-228	153	15	.	.	PUNCT
eurjchem-228	154	1	found	find	VERB
eurjchem-228	154	2	:	:	PUNCT
eurjchem-228	155	1	c	c	X
eurjchem-228	155	2	,	,	PUNCT
eurjchem-228	155	3	73.42	73.42	NUM
eurjchem-228	155	4	;	;	PUNCT
eurjchem-228	155	5	h	h	NOUN
eurjchem-228	155	6	,	,	PUNCT
eurjchem-228	155	7	6.03	6.03	NUM
eurjchem-228	155	8	;	;	PUNCT
eurjchem-228	155	9	n	n	CCONJ
eurjchem-228	155	10	,	,	PUNCT
eurjchem-228	155	11	13.07	13.07	NUM
eurjchem-228	155	12	.	.	X
eurjchem-228	155	13	1‐phenyl‐3‐phenylamino‐propenone	1‐phenyl‐3‐phenylamino‐propenone	NUM
eurjchem-228	155	14	,	,	PUNCT
eurjchem-228	155	15	9c	9c	NUM
eurjchem-228	155	16	:	:	PUNCT
eurjchem-228	155	17	yellow	yellow	ADJ
eurjchem-228	155	18	crystals	crystal	NOUN
eurjchem-228	155	19	.	.	PUNCT
eurjchem-228	156	1	yield	yield	NOUN
eurjchem-228	156	2	:	:	PUNCT
eurjchem-228	156	3	83	83	NUM
eurjchem-228	156	4	%	%	NOUN
eurjchem-228	156	5	.	.	PUNCT
eurjchem-228	157	1	all	all	DET
eurjchem-228	157	2	data	datum	NOUN
eurjchem-228	157	3	agreed	agree	VERB
eurjchem-228	157	4	with	with	ADP
eurjchem-228	157	5	the	the	DET
eurjchem-228	157	6	published	publish	VERB
eurjchem-228	157	7	one	one	NUM
eurjchem-228	157	8	[	[	X
eurjchem-228	157	9	17	17	NUM
eurjchem-228	157	10	]	]	SYM
eurjchem-228	157	11	.	.	PUNCT
eurjchem-228	158	1	170	170	NUM
eurjchem-228	158	2	el‐apasery	el‐apasery	PROPN
eurjchem-228	158	3	et	et	PROPN
eurjchem-228	158	4	al	al	PROPN
eurjchem-228	158	5	.	.	PUNCT
eurjchem-228	158	6	/	/	SYM
eurjchem-228	158	7	european	european	PROPN
eurjchem-228	158	8	journal	journal	PROPN
eurjchem-228	158	9	of	of	ADP
eurjchem-228	158	10	chemistry	chemistry	NOUN
eurjchem-228	158	11	2	2	NUM
eurjchem-228	158	12	(	(	PUNCT
eurjchem-228	158	13	2	2	NUM
eurjchem-228	158	14	)	)	PUNCT
eurjchem-228	158	15	(	(	PUNCT
eurjchem-228	158	16	2011	2011	NUM
eurjchem-228	158	17	)	)	PUNCT
eurjchem-228	158	18	168‐172	168‐172	NUM
eurjchem-228	158	19	table	table	NOUN
eurjchem-228	158	20	1	1	NUM
eurjchem-228	158	21	.	.	PUNCT
eurjchem-228	159	1	crystal	crystal	NOUN
eurjchem-228	159	2	data	datum	NOUN
eurjchem-228	159	3	and	and	CCONJ
eurjchem-228	159	4	structure	structure	NOUN
eurjchem-228	159	5	refinement	refinement	NOUN
eurjchem-228	159	6	for	for	ADP
eurjchem-228	159	7	compound	compound	NOUN
eurjchem-228	159	8	3	3	NUM
eurjchem-228	159	9	.	.	PUNCT
eurjchem-228	159	10	chemical	chemical	ADJ
eurjchem-228	159	11	formula	formula	NOUN
eurjchem-228	159	12	c14h14n2o3	c14h14n2o3	PROPN
eurjchem-228	159	13	formula	formula	VERB
eurjchem-228	159	14	weight	weight	NOUN
eurjchem-228	159	15	258.277	258.277	NUM
eurjchem-228	159	16	crystal	crystal	NOUN
eurjchem-228	159	17	system	system	NOUN
eurjchem-228	159	18	triclinic	triclinic	ADJ
eurjchem-228	159	19	space	space	NOUN
eurjchem-228	159	20	group	group	NOUN
eurjchem-228	159	21	p‐1	p‐1	VERB
eurjchem-228	159	22	a	a	DET
eurjchem-228	159	23	7.9478	7.9478	NUM
eurjchem-228	159	24	(	(	PUNCT
eurjchem-228	159	25	5	5	NUM
eurjchem-228	159	26	)	)	PUNCT
eurjchem-228	159	27	å	å	PROPN
eurjchem-228	159	28	b	b	X
eurjchem-228	159	29	8.4931	8.4931	NUM
eurjchem-228	159	30	(	(	PUNCT
eurjchem-228	159	31	6	6	NUM
eurjchem-228	159	32	)	)	PUNCT
eurjchem-228	159	33	å	å	PROPN
eurjchem-228	159	34	c	c	NOUN
eurjchem-228	159	35	11.1333	11.1333	NUM
eurjchem-228	159	36	(	(	PUNCT
eurjchem-228	159	37	8)	8)	NUM
eurjchem-228	159	38	å	å	PROPN
eurjchem-228	159	39			PROPN
eurjchem-228	159	40	88.231	88.231	NUM
eurjchem-228	159	41	(	(	PUNCT
eurjchem-228	159	42	2	2	NUM
eurjchem-228	159	43	)	)	PUNCT
eurjchem-228	159	44			NOUN
eurjchem-228	159	45			NOUN
eurjchem-228	159	46	83.557	83.557	NUM
eurjchem-228	159	47	(	(	PUNCT
eurjchem-228	159	48	2	2	NUM
eurjchem-228	159	49	)	)	PUNCT
eurjchem-228	159	50			NOUN
eurjchem-228	159	51			NOUN
eurjchem-228	159	52	62.615	62.615	NUM
eurjchem-228	159	53	(	(	PUNCT
eurjchem-228	159	54	2	2	NUM
eurjchem-228	159	55	)	)	PUNCT
eurjchem-228	159	56			NOUN
eurjchem-228	159	57	v	v	ADP
eurjchem-228	159	58	662.90	662.90	NUM
eurjchem-228	159	59	(	(	PUNCT
eurjchem-228	159	60	8)	8)	NUM
eurjchem-228	159	61	å3	å3	PROPN
eurjchem-228	159	62	z	z	NOUN
eurjchem-228	159	63	2	2	NUM
eurjchem-228	159	64	temperature	temperature	NOUN
eurjchem-228	159	65	298	298	NUM
eurjchem-228	159	66	k	k	NOUN
eurjchem-228	159	67	radiation	radiation	NOUN
eurjchem-228	159	68	type	type	NOUN
eurjchem-228	159	69	mo	mo	PROPN
eurjchem-228	159	70	k	k	PROPN
eurjchem-228	159	71	measured	measure	VERB
eurjchem-228	159	72	reflections	reflection	NOUN
eurjchem-228	159	73	3228	3228	NUM
eurjchem-228	159	74	independent	independent	ADJ
eurjchem-228	159	75	reflections	reflection	NOUN
eurjchem-228	159	76	2435	2435	NUM
eurjchem-228	159	77	observed	observe	VERB
eurjchem-228	159	78	reflections	reflection	NOUN
eurjchem-228	159	79	1252	1252	NUM
eurjchem-228	159	80	rint	rint	NOUN
eurjchem-228	159	81	0.036	0.036	NUM
eurjchem-228	159	82	r(all	r(all	NOUN
eurjchem-228	159	83	)	)	PUNCT
eurjchem-228	159	84	0.111	0.111	NUM
eurjchem-228	159	85	r(gt	r(gt	NOUN
eurjchem-228	159	86	)	)	PUNCT
eurjchem-228	159	87	0.064	0.064	NUM
eurjchem-228	159	88	wr(ref	wr(ref	PROPN
eurjchem-228	159	89	)	)	PUNCT
eurjchem-228	159	90	0.119	0.119	NUM
eurjchem-228	159	91	wr(all	wr(all	NOUN
eurjchem-228	159	92	)	)	PUNCT
eurjchem-228	159	93	0.126	0.126	NUM
eurjchem-228	159	94	parameters	parameter	VERB
eurjchem-228	159	95	172	172	NUM
eurjchem-228	159	96	2.6	2.6	NUM
eurjchem-228	159	97	.	.	PUNCT
eurjchem-228	159	98	general	general	ADJ
eurjchem-228	159	99	procedure	procedure	NOUN
eurjchem-228	159	100	for	for	ADP
eurjchem-228	159	101	the	the	DET
eurjchem-228	159	102	synthesis	synthesis	NOUN
eurjchem-228	159	103	of	of	ADP
eurjchem-228	159	104	compounds	compound	NOUN
eurjchem-228	159	105	(	(	PUNCT
eurjchem-228	159	106	12a	12a	NOUN
eurjchem-228	159	107	,	,	PUNCT
eurjchem-228	159	108	b	b	NOUN
eurjchem-228	159	109	)	)	PUNCT
eurjchem-228	159	110	a	a	DET
eurjchem-228	159	111	mixture	mixture	NOUN
eurjchem-228	159	112	of	of	ADP
eurjchem-228	159	113	compound	compound	NOUN
eurjchem-228	159	114	2a‐b	2a‐b	NOUN
eurjchem-228	159	115	(	(	PUNCT
eurjchem-228	159	116	0.01	0.01	NUM
eurjchem-228	159	117	mol	mol	NOUN
eurjchem-228	159	118	)	)	PUNCT
eurjchem-228	159	119	and	and	CCONJ
eurjchem-228	159	120	ammonium	ammonium	NOUN
eurjchem-228	159	121	acetate	acetate	NOUN
eurjchem-228	159	122	(	(	PUNCT
eurjchem-228	159	123	0.2	0.2	NUM
eurjchem-228	159	124	mol	mol	NOUN
eurjchem-228	159	125	)	)	PUNCT
eurjchem-228	159	126	was	be	AUX
eurjchem-228	159	127	irradiated	irradiate	VERB
eurjchem-228	159	128	by	by	ADP
eurjchem-228	159	129	focused	focused	ADJ
eurjchem-228	159	130	microwave	microwave	NOUN
eurjchem-228	159	131	at	at	ADP
eurjchem-228	159	132	160	160	NUM
eurjchem-228	159	133	°	°	ADP
eurjchem-228	159	134	c	c	NOUN
eurjchem-228	159	135	for	for	ADP
eurjchem-228	159	136	10	10	NUM
eurjchem-228	159	137	min	min	NOUN
eurjchem-228	159	138	for	for	ADP
eurjchem-228	159	139	product	product	NOUN
eurjchem-228	159	140	12a	12a	NOUN
eurjchem-228	159	141	,	,	PUNCT
eurjchem-228	159	142	140	140	NUM
eurjchem-228	159	143	°	°	NOUN
eurjchem-228	159	144	c	c	NOUN
eurjchem-228	159	145	for	for	ADP
eurjchem-228	159	146	10	10	NUM
eurjchem-228	159	147	min	min	NOUN
eurjchem-228	159	148	for	for	ADP
eurjchem-228	159	149	product	product	NOUN
eurjchem-228	159	150	12b	12b	NOUN
eurjchem-228	159	151	.	.	PUNCT
eurjchem-228	160	1	completion	completion	NOUN
eurjchem-228	160	2	of	of	ADP
eurjchem-228	160	3	reaction	reaction	NOUN
eurjchem-228	160	4	was	be	AUX
eurjchem-228	160	5	monitored	monitor	VERB
eurjchem-228	160	6	by	by	ADP
eurjchem-228	160	7	tlc	tlc	PROPN
eurjchem-228	160	8	.	.	PUNCT
eurjchem-228	161	1	the	the	DET
eurjchem-228	161	2	solid	solid	ADJ
eurjchem-228	161	3	product	product	NOUN
eurjchem-228	161	4	,	,	PUNCT
eurjchem-228	161	5	so	so	ADV
eurjchem-228	161	6	formed	form	VERB
eurjchem-228	161	7	,	,	PUNCT
eurjchem-228	161	8	was	be	AUX
eurjchem-228	161	9	collected	collect	VERB
eurjchem-228	161	10	and	and	CCONJ
eurjchem-228	161	11	crystallized	crystallize	VERB
eurjchem-228	161	12	from	from	ADP
eurjchem-228	161	13	dioxane	dioxane	NOUN
eurjchem-228	161	14	:	:	PUNCT
eurjchem-228	161	15	etoh	etoh	NOUN
eurjchem-228	161	16	(	(	PUNCT
eurjchem-228	161	17	1:3	1:3	NUM
eurjchem-228	161	18	)	)	PUNCT
eurjchem-228	161	19	to	to	PART
eurjchem-228	161	20	afford	afford	VERB
eurjchem-228	161	21	compounds	compound	NOUN
eurjchem-228	161	22	12a	12a	NOUN
eurjchem-228	161	23	,	,	PUNCT
eurjchem-228	161	24	b.	b.	NOUN
eurjchem-228	162	1	2‐(5‐[2‐(1,3‐dioxo‐2,3‐dihydro‐1h‐2‐isoindolyl)acetyl]‐2‐	2‐(5‐[2‐(1,3‐dioxo‐2,3‐dihydro‐1h‐2‐isoindolyl)acetyl]‐2‐	NUM
eurjchem-228	162	2	pyridylmethyl)‐1,3‐isoindolinedione	pyridylmethyl)‐1,3‐isoindolinedione	NOUN
eurjchem-228	162	3	,	,	PUNCT
eurjchem-228	162	4	12a	12a	NUM
eurjchem-228	162	5	:	:	PUNCT
eurjchem-228	162	6	buff	buff	PROPN
eurjchem-228	162	7	powder	powder	NOUN
eurjchem-228	162	8	.	.	PUNCT
eurjchem-228	163	1	yield	yield	NOUN
eurjchem-228	163	2	:	:	PUNCT
eurjchem-228	163	3	53	53	NUM
eurjchem-228	163	4	%	%	NOUN
eurjchem-228	163	5	.	.	PUNCT
eurjchem-228	164	1	m.p	m.p	PROPN
eurjchem-228	164	2	.	.	PROPN
eurjchem-228	164	3	:	:	PUNCT
eurjchem-228	165	1	235‐236	235‐236	NUM
eurjchem-228	165	2	°	°	SYM
eurjchem-228	165	3	c	c	NOUN
eurjchem-228	165	4	.	.	PUNCT
eurjchem-228	166	1	ft‐ir	ft‐ir	NOUN
eurjchem-228	166	2	(	(	PUNCT
eurjchem-228	166	3	kbr	kbr	PROPN
eurjchem-228	166	4	,	,	PUNCT
eurjchem-228	166	5	cm‐1	cm‐1	PROPN
eurjchem-228	166	6	):	):	PUNCT
eurjchem-228	166	7	1714	1714	NUM
eurjchem-228	166	8	(	(	PUNCT
eurjchem-228	166	9	co	co	NOUN
eurjchem-228	166	10	)	)	PUNCT
eurjchem-228	166	11	.	.	PUNCT
eurjchem-228	167	1	1h	1h	NUM
eurjchem-228	167	2	nmr	nmr	NOUN
eurjchem-228	167	3	(	(	PUNCT
eurjchem-228	167	4	400	400	NUM
eurjchem-228	167	5	mhz	mhz	NOUN
eurjchem-228	167	6	,	,	PUNCT
eurjchem-228	167	7	dmso‐d6	dmso‐d6	NUM
eurjchem-228	167	8	):	):	PUNCT
eurjchem-228	167	9	5.04	5.04	NUM
eurjchem-228	167	10	(	(	PUNCT
eurjchem-228	167	11	s	s	PROPN
eurjchem-228	167	12	,	,	PUNCT
eurjchem-228	167	13	2h	2h	NUM
eurjchem-228	167	14	,	,	PUNCT
eurjchem-228	167	15	ch2	ch2	PROPN
eurjchem-228	167	16	)	)	PUNCT
eurjchem-228	167	17	,	,	PUNCT
eurjchem-228	167	18	5.29	5.29	NUM
eurjchem-228	167	19	(	(	PUNCT
eurjchem-228	167	20	s	s	PROPN
eurjchem-228	167	21	,	,	PUNCT
eurjchem-228	167	22	2h	2h	NUM
eurjchem-228	167	23	,	,	PUNCT
eurjchem-228	167	24	ch2	ch2	PROPN
eurjchem-228	167	25	)	)	PUNCT
eurjchem-228	167	26	,	,	PUNCT
eurjchem-228	167	27	7.23	7.23	NUM
eurjchem-228	167	28	(	(	PUNCT
eurjchem-228	167	29	d	d	PROPN
eurjchem-228	167	30	,	,	PUNCT
eurjchem-228	167	31	1h	1h	NUM
eurjchem-228	167	32	,	,	PUNCT
eurjchem-228	167	33	j=7.6	j=7.6	NOUN
eurjchem-228	167	34	hz	hz	VERB
eurjchem-228	167	35	,	,	PUNCT
eurjchem-228	167	36	ar‐h	ar‐h	PROPN
eurjchem-228	167	37	)	)	PUNCT
eurjchem-228	167	38	,	,	PUNCT
eurjchem-228	167	39	7.59‐7.63	7.59‐7.63	NUM
eurjchem-228	167	40	(	(	PUNCT
eurjchem-228	167	41	m	m	PROPN
eurjchem-228	167	42	,	,	PUNCT
eurjchem-228	167	43	1h	1h	NUM
eurjchem-228	167	44	,	,	PUNCT
eurjchem-228	167	45	ar‐h	ar‐h	NOUN
eurjchem-228	167	46	)	)	PUNCT
eurjchem-228	167	47	,	,	PUNCT
eurjchem-228	167	48	7.31	7.31	NUM
eurjchem-228	167	49	(	(	PUNCT
eurjchem-228	167	50	d	d	PROPN
eurjchem-228	167	51	,	,	PUNCT
eurjchem-228	167	52	1h	1h	NUM
eurjchem-228	167	53	,	,	PUNCT
eurjchem-228	167	54	j=8.4	j=8.4	NOUN
eurjchem-228	167	55	hz	hz	VERB
eurjchem-228	167	56	,	,	PUNCT
eurjchem-228	167	57	ar‐h	ar‐h	PROPN
eurjchem-228	167	58	)	)	PUNCT
eurjchem-228	167	59	,	,	PUNCT
eurjchem-228	168	1	7.76‐7.81	7.76‐7.81	NUM
eurjchem-228	168	2	(	(	PUNCT
eurjchem-228	168	3	m	m	PROPN
eurjchem-228	168	4	,	,	PUNCT
eurjchem-228	168	5	1h	1h	NUM
eurjchem-228	168	6	,	,	PUNCT
eurjchem-228	168	7	ar‐h	ar‐h	NOUN
eurjchem-228	168	8	)	)	PUNCT
eurjchem-228	168	9	.	.	PUNCT
eurjchem-228	169	1	7.87	7.87	NUM
eurjchem-228	169	2	(	(	PUNCT
eurjchem-228	169	3	s	s	PROPN
eurjchem-228	169	4	,	,	PUNCT
eurjchem-228	169	5	1h	1h	NUM
eurjchem-228	169	6	,	,	PUNCT
eurjchem-228	169	7	ar‐h	ar‐h	NOUN
eurjchem-228	169	8	)	)	PUNCT
eurjchem-228	169	9	,	,	PUNCT
eurjchem-228	169	10	7.98‐8.00	7.98‐8.00	NUM
eurjchem-228	169	11	(	(	PUNCT
eurjchem-228	169	12	m	m	PROPN
eurjchem-228	169	13	,	,	PUNCT
eurjchem-228	169	14	4h	4h	NOUN
eurjchem-228	169	15	,	,	PUNCT
eurjchem-228	169	16	ar‐h	ar‐h	PROPN
eurjchem-228	169	17	)	)	PUNCT
eurjchem-228	169	18	,	,	PUNCT
eurjchem-228	169	19	7.31	7.31	NUM
eurjchem-228	169	20	(	(	PUNCT
eurjchem-228	169	21	dd	dd	PROPN
eurjchem-228	169	22	,	,	PUNCT
eurjchem-228	169	23	1h	1h	NUM
eurjchem-228	169	24	,	,	PUNCT
eurjchem-228	169	25	j=2.4	j=2.4	PROPN
eurjchem-228	169	26	hz	hz	PART
eurjchem-228	169	27	,	,	PUNCT
eurjchem-228	169	28	j=2.0	j=2.0	PROPN
eurjchem-228	169	29	hz	hz	PROPN
eurjchem-228	169	30	,	,	PUNCT
eurjchem-228	169	31	ar‐h	ar‐h	PROPN
eurjchem-228	169	32	)	)	PUNCT
eurjchem-228	169	33	,	,	PUNCT
eurjchem-228	169	34	9.15	9.15	NUM
eurjchem-228	169	35	(	(	PUNCT
eurjchem-228	169	36	s	s	PROPN
eurjchem-228	169	37	,	,	PUNCT
eurjchem-228	169	38	1h	1h	NUM
eurjchem-228	169	39	,	,	PUNCT
eurjchem-228	169	40	ar‐h	ar‐h	NOUN
eurjchem-228	169	41	)	)	PUNCT
eurjchem-228	169	42	.	.	PUNCT
eurjchem-228	170	1	ms	ms	NOUN
eurjchem-228	170	2	(	(	PUNCT
eurjchem-228	170	3	ei	ei	PROPN
eurjchem-228	170	4	,	,	PUNCT
eurjchem-228	170	5	m	m	PROPN
eurjchem-228	170	6	/	/	SYM
eurjchem-228	170	7	z	z	NOUN
eurjchem-228	170	8	,	,	PUNCT
eurjchem-228	170	9	%	%	INTJ
eurjchem-228	170	10	):	):	PUNCT
eurjchem-228	170	11	425	425	NUM
eurjchem-228	170	12	[	[	X
eurjchem-228	170	13	m+	m+	NUM
eurjchem-228	170	14	,	,	PUNCT
eurjchem-228	170	15	10	10	NUM
eurjchem-228	170	16	%	%	NOUN
eurjchem-228	170	17	]	]	PUNCT
eurjchem-228	170	18	.	.	PUNCT
eurjchem-228	171	1	anal	anal	ADJ
eurjchem-228	171	2	.	.	PUNCT
eurjchem-228	171	3	calcd	calcd	NOUN
eurjchem-228	171	4	.	.	PUNCT
eurjchem-228	172	1	for	for	ADP
eurjchem-228	172	2	c24h15n3o5	c24h15n3o5	NOUN
eurjchem-228	172	3	:	:	PUNCT
eurjchem-228	172	4	c	c	X
eurjchem-228	172	5	,	,	PUNCT
eurjchem-228	172	6	67.76	67.76	NUM
eurjchem-228	172	7	;	;	PUNCT
eurjchem-228	172	8	h	h	X
eurjchem-228	172	9	,	,	PUNCT
eurjchem-228	172	10	3.55	3.55	NUM
eurjchem-228	172	11	;	;	PUNCT
eurjchem-228	172	12	n	n	CCONJ
eurjchem-228	172	13	,	,	PUNCT
eurjchem-228	172	14	9.88	9.88	NUM
eurjchem-228	172	15	.	.	PUNCT
eurjchem-228	172	16	found	find	VERB
eurjchem-228	172	17	:	:	PUNCT
eurjchem-228	173	1	c	c	X
eurjchem-228	173	2	,	,	PUNCT
eurjchem-228	173	3	67.70	67.70	NUM
eurjchem-228	173	4	;	;	PUNCT
eurjchem-228	173	5	h	h	NOUN
eurjchem-228	173	6	,	,	PUNCT
eurjchem-228	173	7	3.63	3.63	NUM
eurjchem-228	173	8	;	;	PUNCT
eurjchem-228	173	9	n	n	CCONJ
eurjchem-228	173	10	,	,	PUNCT
eurjchem-228	173	11	9.77	9.77	NUM
eurjchem-228	173	12	.	.	PUNCT
eurjchem-228	174	1	1h‐2‐pyrrolyl[6‐(1h‐2‐pyrrolyl)‐3‐pyridyl]methanone	1h‐2‐pyrrolyl[6‐(1h‐2‐pyrrolyl)‐3‐pyridyl]methanone	NUM
eurjchem-228	174	2	,	,	PUNCT
eurjchem-228	174	3	12b	12b	NOUN
eurjchem-228	174	4	:	:	PUNCT
eurjchem-228	174	5	brown	brown	ADJ
eurjchem-228	174	6	powder	powder	NOUN
eurjchem-228	174	7	.	.	PUNCT
eurjchem-228	174	8	yield	yield	NOUN
eurjchem-228	174	9	:	:	PUNCT
eurjchem-228	174	10	78	78	NUM
eurjchem-228	174	11	%	%	NOUN
eurjchem-228	174	12	.	.	PUNCT
eurjchem-228	175	1	m.p	m.p	PROPN
eurjchem-228	175	2	.	.	PROPN
eurjchem-228	175	3	:	:	PUNCT
eurjchem-228	176	1	136‐137	136‐137	NUM
eurjchem-228	176	2	°	°	SYM
eurjchem-228	176	3	c	c	X
eurjchem-228	176	4	.	.	PUNCT
eurjchem-228	177	1	ft‐ir	ft‐ir	NOUN
eurjchem-228	177	2	(	(	PUNCT
eurjchem-228	177	3	kbr	kbr	PROPN
eurjchem-228	177	4	,	,	PUNCT
eurjchem-228	177	5	cm‐1	cm‐1	PROPN
eurjchem-228	177	6	):	):	PUNCT
eurjchem-228	177	7	3295	3295	NUM
eurjchem-228	177	8	(	(	PUNCT
eurjchem-228	177	9	nh	nh	NOUN
eurjchem-228	177	10	)	)	PUNCT
eurjchem-228	177	11	,	,	PUNCT
eurjchem-228	177	12	1618	1618	NUM
eurjchem-228	177	13	(	(	PUNCT
eurjchem-228	177	14	co	co	NOUN
eurjchem-228	177	15	)	)	PUNCT
eurjchem-228	177	16	.	.	PUNCT
eurjchem-228	178	1	1h	1h	NUM
eurjchem-228	178	2	nmr	nmr	NOUN
eurjchem-228	178	3	(	(	PUNCT
eurjchem-228	178	4	400	400	NUM
eurjchem-228	178	5	mhz	mhz	NOUN
eurjchem-228	178	6	,	,	PUNCT
eurjchem-228	178	7	dmso‐d6	dmso‐d6	NUM
eurjchem-228	178	8	):	):	PUNCT
eurjchem-228	178	9	6.31	6.31	NUM
eurjchem-228	178	10	(	(	PUNCT
eurjchem-228	178	11	t	t	PROPN
eurjchem-228	178	12	,	,	PUNCT
eurjchem-228	178	13	1h	1h	NUM
eurjchem-228	178	14	,	,	PUNCT
eurjchem-228	178	15	j=4.0	j=4.0	PROPN
eurjchem-228	178	16	hz	hz	NOUN
eurjchem-228	178	17	,	,	PUNCT
eurjchem-228	178	18	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	178	19	)	)	PUNCT
eurjchem-228	178	20	,	,	PUNCT
eurjchem-228	178	21	6.92	6.92	NUM
eurjchem-228	178	22	(	(	PUNCT
eurjchem-228	178	23	t	t	PROPN
eurjchem-228	178	24	,	,	PUNCT
eurjchem-228	178	25	1h	1h	NUM
eurjchem-228	178	26	,	,	PUNCT
eurjchem-228	178	27	j=2.8	j=2.8	PROPN
eurjchem-228	178	28	hz	hz	NOUN
eurjchem-228	178	29	,	,	PUNCT
eurjchem-228	178	30	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	178	31	)	)	PUNCT
eurjchem-228	178	32	,	,	PUNCT
eurjchem-228	178	33	7.30	7.30	NUM
eurjchem-228	178	34	(	(	PUNCT
eurjchem-228	178	35	d	d	PROPN
eurjchem-228	178	36	,	,	PUNCT
eurjchem-228	178	37	1h	1h	NUM
eurjchem-228	178	38	,	,	PUNCT
eurjchem-228	178	39	j=9.2	j=9.2	NOUN
eurjchem-228	178	40	hz	hz	NOUN
eurjchem-228	178	41	,	,	PUNCT
eurjchem-228	178	42	pyrrolyl‐h	pyrrolyl‐h	PROPN
eurjchem-228	178	43	)	)	PUNCT
eurjchem-228	178	44	,	,	PUNCT
eurjchem-228	178	45	8.41(d	8.41(d	NUM
eurjchem-228	178	46	,	,	PUNCT
eurjchem-228	178	47	2h	2h	NUM
eurjchem-228	178	48	,	,	PUNCT
eurjchem-228	178	49	j=4.8	j=4.8	NOUN
eurjchem-228	178	50	hz	hz	NOUN
eurjchem-228	178	51	,	,	PUNCT
eurjchem-228	178	52	pyridinyl‐h	pyridinyl‐h	NOUN
eurjchem-228	178	53	)	)	PUNCT
eurjchem-228	178	54	,	,	PUNCT
eurjchem-228	178	55	9.14	9.14	NUM
eurjchem-228	178	56	(	(	PUNCT
eurjchem-228	178	57	s	s	PROPN
eurjchem-228	178	58	,	,	PUNCT
eurjchem-228	178	59	1h	1h	NUM
eurjchem-228	178	60	,	,	PUNCT
eurjchem-228	178	61	pyridinyl‐h	pyridinyl‐h	NOUN
eurjchem-228	178	62	)	)	PUNCT
eurjchem-228	178	63	,	,	PUNCT
eurjchem-228	178	64	12.28	12.28	NUM
eurjchem-228	178	65	(	(	PUNCT
eurjchem-228	178	66	s	s	PROPN
eurjchem-228	178	67	,	,	PUNCT
eurjchem-228	178	68	2h	2h	NUM
eurjchem-228	178	69	,	,	PUNCT
eurjchem-228	178	70	nh	nh	PROPN
eurjchem-228	178	71	)	)	PUNCT
eurjchem-228	178	72	.	.	PUNCT
eurjchem-228	179	1	ms	ms	NOUN
eurjchem-228	179	2	(	(	PUNCT
eurjchem-228	179	3	ei	ei	PROPN
eurjchem-228	179	4	,	,	PUNCT
eurjchem-228	179	5	m	m	PROPN
eurjchem-228	179	6	/	/	SYM
eurjchem-228	179	7	z	z	NOUN
eurjchem-228	179	8	,	,	PUNCT
eurjchem-228	179	9	%	%	INTJ
eurjchem-228	179	10	):	):	PUNCT
eurjchem-228	179	11	237	237	NUM
eurjchem-228	180	1	[	[	X
eurjchem-228	180	2	m+	m+	NUM
eurjchem-228	180	3	,	,	PUNCT
eurjchem-228	180	4	100	100	NUM
eurjchem-228	180	5	%	%	NOUN
eurjchem-228	180	6	]	]	PUNCT
eurjchem-228	180	7	.	.	PUNCT
eurjchem-228	181	1	anal	anal	ADJ
eurjchem-228	181	2	.	.	PUNCT
eurjchem-228	181	3	calcd	calcd	NOUN
eurjchem-228	181	4	.	.	PUNCT
eurjchem-228	182	1	for	for	ADP
eurjchem-228	182	2	c14h11n3o	c14h11n3o	NOUN
eurjchem-228	182	3	:	:	PUNCT
eurjchem-228	182	4	c	c	X
eurjchem-228	182	5	,	,	PUNCT
eurjchem-228	182	6	70.87	70.87	NUM
eurjchem-228	182	7	;	;	PUNCT
eurjchem-228	182	8	h	h	NOUN
eurjchem-228	182	9	,	,	PUNCT
eurjchem-228	182	10	4.67	4.67	NUM
eurjchem-228	182	11	;	;	PUNCT
eurjchem-228	182	12	n	n	CCONJ
eurjchem-228	182	13	,	,	PUNCT
eurjchem-228	182	14	17.71	17.71	NUM
eurjchem-228	182	15	.	.	PUNCT
eurjchem-228	182	16	found	find	VERB
eurjchem-228	182	17	:	:	PUNCT
eurjchem-228	183	1	c	c	X
eurjchem-228	183	2	,	,	PUNCT
eurjchem-228	183	3	69.87	69.87	NUM
eurjchem-228	183	4	;	;	PUNCT
eurjchem-228	183	5	h	h	X
eurjchem-228	183	6	,	,	PUNCT
eurjchem-228	183	7	4.66	4.66	NUM
eurjchem-228	183	8	;	;	PUNCT
eurjchem-228	183	9	n	n	CCONJ
eurjchem-228	183	10	,	,	PUNCT
eurjchem-228	183	11	17.53	17.53	NUM
eurjchem-228	183	12	.	.	NOUN
eurjchem-228	184	1	3	3	NUM
eurjchem-228	184	2	.	.	NOUN
eurjchem-228	184	3	results	result	NOUN
eurjchem-228	184	4	and	and	CCONJ
eurjchem-228	184	5	discussion	discussion	NOUN
eurjchem-228	184	6	condensation	condensation	NOUN
eurjchem-228	184	7	of	of	ADP
eurjchem-228	184	8	phthalimidoacetone	phthalimidoacetone	NOUN
eurjchem-228	184	9	1a	1a	NOUN
eurjchem-228	184	10	with	with	ADP
eurjchem-228	184	11	dimethyl	dimethyl	PROPN
eurjchem-228	184	12	formamide	formamide	PROPN
eurjchem-228	184	13	dimethyl	dimethyl	PROPN
eurjchem-228	184	14	acetal	acetal	NOUN
eurjchem-228	184	15	(	(	PUNCT
eurjchem-228	184	16	dmf‐dma	dmf‐dma	NOUN
eurjchem-228	184	17	)	)	PUNCT
eurjchem-228	184	18	has	have	AUX
eurjchem-228	184	19	afforded	afford	VERB
eurjchem-228	184	20	enaminone	enaminone	NOUN
eurjchem-228	184	21	2a	2a	NUM
eurjchem-228	184	22	in	in	ADP
eurjchem-228	184	23	focused	focused	ADJ
eurjchem-228	184	24	microwave	microwave	NOUN
eurjchem-228	184	25	oven	oven	NOUN
eurjchem-228	184	26	at	at	ADP
eurjchem-228	184	27	180	180	NUM
eurjchem-228	184	28	°	°	NOUN
eurjchem-228	184	29	c	c	NOUN
eurjchem-228	184	30	for	for	ADP
eurjchem-228	184	31	20	20	NUM
eurjchem-228	184	32	min	min	NOUN
eurjchem-228	184	33	in	in	ADP
eurjchem-228	184	34	absence	absence	NOUN
eurjchem-228	184	35	of	of	ADP
eurjchem-228	184	36	solvent	solvent	NOUN
eurjchem-228	184	37	in	in	ADP
eurjchem-228	184	38	77	77	NUM
eurjchem-228	184	39	%	%	NOUN
eurjchem-228	184	40	yield	yield	NOUN
eurjchem-228	184	41	.	.	PUNCT
eurjchem-228	185	1	also	also	ADV
eurjchem-228	185	2	,	,	PUNCT
eurjchem-228	185	3	a	a	DET
eurjchem-228	185	4	side	side	NOUN
eurjchem-228	185	5	product	product	NOUN
eurjchem-228	185	6	was	be	AUX
eurjchem-228	185	7	isolated	isolate	VERB
eurjchem-228	185	8	from	from	ADP
eurjchem-228	185	9	this	this	DET
eurjchem-228	185	10	reaction	reaction	NOUN
eurjchem-228	185	11	.	.	PUNCT
eurjchem-228	186	1	isolation	isolation	NOUN
eurjchem-228	186	2	of	of	ADP
eurjchem-228	186	3	the	the	DET
eurjchem-228	186	4	side	side	NOUN
eurjchem-228	186	5	product	product	NOUN
eurjchem-228	186	6	has	have	AUX
eurjchem-228	186	7	not	not	PART
eurjchem-228	186	8	been	be	AUX
eurjchem-228	186	9	observed	observe	VERB
eurjchem-228	186	10	earlier	early	ADV
eurjchem-228	186	11	.	.	PUNCT
eurjchem-228	187	1	the	the	DET
eurjchem-228	187	2	x‐ray	x‐ray	PROPN
eurjchem-228	187	3	crystal	crystal	NOUN
eurjchem-228	187	4	structure	structure	NOUN
eurjchem-228	187	5	for	for	ADP
eurjchem-228	187	6	this	this	DET
eurjchem-228	187	7	product	product	NOUN
eurjchem-228	187	8	indicated	indicate	VERB
eurjchem-228	187	9	that	that	SCONJ
eurjchem-228	187	10	it	it	PRON
eurjchem-228	187	11	resulted	result	VERB
eurjchem-228	187	12	from	from	ADP
eurjchem-228	187	13	condensation	condensation	NOUN
eurjchem-228	187	14	of	of	ADP
eurjchem-228	187	15	methylene	methylene	ADJ
eurjchem-228	187	16	moiety	moiety	NOUN
eurjchem-228	187	17	in	in	ADP
eurjchem-228	187	18	1a	1a	NOUN
eurjchem-228	187	19	with	with	ADP
eurjchem-228	187	20	dmf‐dma	dmf‐dma	NOUN
eurjchem-228	187	21	to	to	PART
eurjchem-228	187	22	yield	yield	VERB
eurjchem-228	187	23	2‐(1‐	2‐(1‐	PROPN
eurjchem-228	187	24	dimethylamino	dimethylamino	PROPN
eurjchem-228	187	25	methylene‐2‐oxo‐propyl)isoindole‐1,3‐dione	methylene‐2‐oxo‐propyl)isoindole‐1,3‐dione	NOUN
eurjchem-228	187	26	(	(	PUNCT
eurjchem-228	187	27	3	3	NUM
eurjchem-228	187	28	)	)	PUNCT
eurjchem-228	187	29	(	(	PUNCT
eurjchem-228	187	30	figure	figure	NOUN
eurjchem-228	187	31	1	1	NUM
eurjchem-228	187	32	)	)	PUNCT
eurjchem-228	187	33	.	.	PUNCT
eurjchem-228	188	1	in	in	ADP
eurjchem-228	188	2	table	table	NOUN
eurjchem-228	188	3	2	2	NUM
eurjchem-228	188	4	,	,	PUNCT
eurjchem-228	188	5	we	we	PRON
eurjchem-228	188	6	list	list	VERB
eurjchem-228	188	7	the	the	DET
eurjchem-228	188	8	selected	select	VERB
eurjchem-228	188	9	bond	bond	NOUN
eurjchem-228	188	10	lengths	length	NOUN
eurjchem-228	188	11	and	and	CCONJ
eurjchem-228	188	12	angles	angle	NOUN
eurjchem-228	188	13	for	for	ADP
eurjchem-228	188	14	compound	compound	NOUN
eurjchem-228	188	15	3	3	NUM
eurjchem-228	188	16	.	.	PUNCT
eurjchem-228	189	1	it	it	PRON
eurjchem-228	189	2	is	be	AUX
eurjchem-228	189	3	clear	clear	ADJ
eurjchem-228	189	4	from	from	ADP
eurjchem-228	189	5	figure	figure	NOUN
eurjchem-228	189	6	1	1	NUM
eurjchem-228	189	7	that	that	SCONJ
eurjchem-228	189	8	the	the	DET
eurjchem-228	189	9	product	product	NOUN
eurjchem-228	189	10	adopted	adopt	VERB
eurjchem-228	189	11	sterical	sterical	ADJ
eurjchem-228	189	12	strained	strained	ADJ
eurjchem-228	189	13	form	form	NOUN
eurjchem-228	189	14	compound	compound	VERB
eurjchem-228	189	15	3	3	NUM
eurjchem-228	189	16	rather	rather	ADV
eurjchem-228	189	17	than	than	ADP
eurjchem-228	189	18	compound	compound	VERB
eurjchem-228	189	19	3a	3a	NUM
eurjchem-228	189	20	.	.	PUNCT
eurjchem-228	190	1	this	this	PRON
eurjchem-228	190	2	is	be	AUX
eurjchem-228	190	3	a	a	DET
eurjchem-228	190	4	further	further	ADJ
eurjchem-228	190	5	example	example	NOUN
eurjchem-228	190	6	indicating	indicate	VERB
eurjchem-228	190	7	that	that	SCONJ
eurjchem-228	190	8	steroelectronic	steroelectronic	ADJ
eurjchem-228	190	9	factors	factor	NOUN
eurjchem-228	190	10	overweight	overweight	VERB
eurjchem-228	190	11	steric	steric	ADJ
eurjchem-228	190	12	factors	factor	NOUN
eurjchem-228	190	13	.	.	PUNCT
eurjchem-228	191	1	it	it	PRON
eurjchem-228	191	2	has	have	AUX
eurjchem-228	191	3	previously	previously	ADV
eurjchem-228	191	4	indicated	indicate	VERB
eurjchem-228	191	5	that	that	SCONJ
eurjchem-228	191	6	this	this	PRON
eurjchem-228	191	7	is	be	AUX
eurjchem-228	191	8	the	the	DET
eurjchem-228	191	9	case	case	NOUN
eurjchem-228	191	10	when	when	SCONJ
eurjchem-228	191	11	steroelectronic	steroelectronic	ADJ
eurjchem-228	191	12	factors	factor	NOUN
eurjchem-228	191	13	and	and	CCONJ
eurjchem-228	191	14	steric	steric	ADJ
eurjchem-228	191	15	factors	factor	NOUN
eurjchem-228	191	16	contradict	contradict	VERB
eurjchem-228	191	17	[	[	X
eurjchem-228	191	18	18	18	NUM
eurjchem-228	191	19	]	]	PUNCT
eurjchem-228	191	20	.	.	PUNCT
eurjchem-228	192	1	bond	bond	NOUN
eurjchem-228	192	2	length	length	NOUN
eurjchem-228	192	3	for	for	ADP
eurjchem-228	192	4	n2‐c15	n2‐c15	NOUN
eurjchem-228	192	5	is	be	AUX
eurjchem-228	192	6	typical	typical	ADJ
eurjchem-228	192	7	for	for	ADP
eurjchem-228	192	8	n‐c	n‐c	PROPN
eurjchem-228	192	9	single	single	ADJ
eurjchem-228	192	10	bond	bond	NOUN
eurjchem-228	192	11	.	.	PUNCT
eurjchem-228	193	1	the	the	DET
eurjchem-228	193	2	same	same	ADJ
eurjchem-228	193	3	applies	apply	VERB
eurjchem-228	193	4	for	for	ADP
eurjchem-228	193	5	n5	n5	PROPN
eurjchem-228	193	6	and	and	CCONJ
eurjchem-228	193	7	c7	c7	PROPN
eurjchem-228	193	8	indicating	indicate	VERB
eurjchem-228	193	9	that	that	SCONJ
eurjchem-228	193	10	charge	charge	NOUN
eurjchem-228	193	11	separated	separate	VERB
eurjchem-228	193	12	resonance	resonance	NOUN
eurjchem-228	193	13	form	form	NOUN
eurjchem-228	193	14	3a	3a	NUM
eurjchem-228	193	15	does	do	AUX
eurjchem-228	193	16	play	play	VERB
eurjchem-228	193	17	significant	significant	ADJ
eurjchem-228	193	18	role	role	NOUN
eurjchem-228	193	19	.	.	PUNCT
eurjchem-228	194	1	heating	heating	NOUN
eurjchem-228	194	2	of	of	ADP
eurjchem-228	194	3	methyl	methyl	NOUN
eurjchem-228	194	4	ketones	ketone	NOUN
eurjchem-228	194	5	1b	1b	NUM
eurjchem-228	194	6	,	,	PUNCT
eurjchem-228	194	7	c	c	NOUN
eurjchem-228	194	8	with	with	ADP
eurjchem-228	194	9	(	(	PUNCT
eurjchem-228	194	10	dmf‐dma	dmf‐dma	NOUN
eurjchem-228	194	11	)	)	PUNCT
eurjchem-228	194	12	in	in	ADP
eurjchem-228	194	13	mw	mw	NOUN
eurjchem-228	194	14	with	with	ADP
eurjchem-228	194	15	solvent‐free	solvent‐free	NOUN
eurjchem-228	194	16	at	at	ADP
eurjchem-228	194	17	120	120	NUM
eurjchem-228	194	18	°	°	NOUN
eurjchem-228	194	19	c	c	NOUN
eurjchem-228	194	20	for	for	ADP
eurjchem-228	194	21	10‐30	10‐30	PROPN
eurjchem-228	194	22	min	min	PROPN
eurjchem-228	194	23	has	have	AUX
eurjchem-228	194	24	afforded	afford	VERB
eurjchem-228	194	25	enaminones	enaminone	NOUN
eurjchem-228	194	26	2b	2b	NOUN
eurjchem-228	194	27	,	,	PUNCT
eurjchem-228	194	28	c	c	NOUN
eurjchem-228	194	29	in	in	ADP
eurjchem-228	194	30	86	86	NUM
eurjchem-228	194	31	%	%	NOUN
eurjchem-228	194	32	and	and	CCONJ
eurjchem-228	194	33	87	87	NUM
eurjchem-228	194	34	%	%	NOUN
eurjchem-228	194	35	yields	yield	NOUN
eurjchem-228	194	36	,	,	PUNCT
eurjchem-228	194	37	respectively	respectively	ADV
eurjchem-228	194	38	.	.	PUNCT
eurjchem-228	195	1	recently	recently	ADV
eurjchem-228	195	2	,	,	PUNCT
eurjchem-228	195	3	it	it	PRON
eurjchem-228	195	4	was	be	AUX
eurjchem-228	195	5	reported	report	VERB
eurjchem-228	195	6	that	that	SCONJ
eurjchem-228	195	7	heating	heating	NOUN
eurjchem-228	195	8	neat	neat	ADJ
eurjchem-228	195	9	reactants	reactant	NOUN
eurjchem-228	195	10	in	in	ADP
eurjchem-228	195	11	ionic	ionic	ADJ
eurjchem-228	195	12	liquid	liquid	NOUN
eurjchem-228	195	13	afforded	afford	VERB
eurjchem-228	195	14	compounds	compound	NOUN
eurjchem-228	195	15	2b	2b	NOUN
eurjchem-228	195	16	,	,	PUNCT
eurjchem-228	195	17	c	c	NOUN
eurjchem-228	195	18	in	in	ADP
eurjchem-228	195	19	86	86	NUM
eurjchem-228	195	20	%	%	NOUN
eurjchem-228	195	21	and	and	CCONJ
eurjchem-228	195	22	70	70	NUM
eurjchem-228	195	23	%	%	NOUN
eurjchem-228	195	24	yields	yield	NOUN
eurjchem-228	195	25	,	,	PUNCT
eurjchem-228	195	26	respectively	respectively	ADV
eurjchem-228	195	27	[	[	X
eurjchem-228	195	28	19	19	NUM
eurjchem-228	195	29	]	]	PUNCT
eurjchem-228	195	30	(	(	PUNCT
eurjchem-228	195	31	scheme	scheme	NOUN
eurjchem-228	195	32	1	1	NUM
eurjchem-228	195	33	)	)	PUNCT
eurjchem-228	195	34	.	.	PUNCT
eurjchem-228	196	1	figure	figure	NOUN
eurjchem-228	196	2	1	1	NUM
eurjchem-228	196	3	.	.	PUNCT
eurjchem-228	197	1	x‐ray	x‐ray	PROPN
eurjchem-228	197	2	crystal	crystal	NOUN
eurjchem-228	197	3	structure	structure	NOUN
eurjchem-228	197	4	of	of	ADP
eurjchem-228	197	5	compound	compound	NOUN
eurjchem-228	197	6	(	(	PUNCT
eurjchem-228	197	7	3	3	NUM
eurjchem-228	197	8	)	)	PUNCT
eurjchem-228	197	9	.	.	PUNCT
eurjchem-228	198	1	table	table	NOUN
eurjchem-228	198	2	2	2	NUM
eurjchem-228	198	3	.	.	NUM
eurjchem-228	198	4	selected	select	VERB
eurjchem-228	198	5	bond	bond	NOUN
eurjchem-228	198	6	lengths	length	NOUN
eurjchem-228	198	7	and	and	CCONJ
eurjchem-228	198	8	angles	angle	NOUN
eurjchem-228	198	9	for	for	ADP
eurjchem-228	198	10	compound	compound	NOUN
eurjchem-228	198	11	3	3	NUM
eurjchem-228	198	12	.	.	PUNCT
eurjchem-228	199	1	bond	bond	NOUN
eurjchem-228	199	2	bond	bond	NOUN
eurjchem-228	199	3	length	length	NOUN
eurjchem-228	199	4	(	(	PUNCT
eurjchem-228	199	5	å	å	NOUN
eurjchem-228	199	6	)	)	PUNCT
eurjchem-228	199	7	bond	bond	NOUN
eurjchem-228	199	8	bond	bond	NOUN
eurjchem-228	199	9	angle	angle	NOUN
eurjchem-228	199	10	(	(	PUNCT
eurjchem-228	199	11	°	°	PROPN
eurjchem-228	199	12	)	)	PUNCT
eurjchem-228	199	13	n2‐c6	n2‐c6	VERB
eurjchem-228	199	14	1.397	1.397	NUM
eurjchem-228	199	15	(	(	PUNCT
eurjchem-228	199	16	6	6	NUM
eurjchem-228	199	17	)	)	PUNCT
eurjchem-228	199	18	c7‐n5‐c17	c7‐n5‐c17	ADP
eurjchem-228	199	19	120.0	120.0	NUM
eurjchem-228	199	20	(	(	PUNCT
eurjchem-228	199	21	4	4	NUM
eurjchem-228	199	22	)	)	PUNCT
eurjchem-228	199	23	n2‐c13	n2‐c13	X
eurjchem-228	199	24	1.414	1.414	NUM
eurjchem-228	199	25	(	(	PUNCT
eurjchem-228	199	26	6	6	NUM
eurjchem-228	199	27	)	)	PUNCT
eurjchem-228	199	28	n2‐c15‐c7	n2‐c15‐c7	ADP
eurjchem-228	199	29	123.5	123.5	NUM
eurjchem-228	199	30	(	(	PUNCT
eurjchem-228	199	31	3	3	NUM
eurjchem-228	199	32	)	)	PUNCT
eurjchem-228	199	33	n2‐c15	n2‐c15	NOUN
eurjchem-228	199	34	1.434	1.434	NUM
eurjchem-228	199	35	(	(	PUNCT
eurjchem-228	199	36	5	5	NUM
eurjchem-228	199	37	)	)	PUNCT
eurjchem-228	199	38	c7‐c15‐c9	c7‐c15‐c9	PROPN
eurjchem-228	199	39	121.8	121.8	NUM
eurjchem-228	199	40	(	(	PUNCT
eurjchem-228	199	41	4	4	NUM
eurjchem-228	199	42	)	)	PUNCT
eurjchem-228	199	43	n5‐c7	n5‐c7	NOUN
eurjchem-228	199	44	1.339	1.339	NUM
eurjchem-228	199	45	(	(	PUNCT
eurjchem-228	199	46	6	6	NUM
eurjchem-228	199	47	)	)	PUNCT
eurjchem-228	199	48	n5‐c7‐c15	n5‐c7‐c15	ADP
eurjchem-228	199	49	33.3	33.3	NUM
eurjchem-228	199	50	(	(	PUNCT
eurjchem-228	199	51	4	4	NUM
eurjchem-228	199	52	)	)	PUNCT
eurjchem-228	199	53	n5‐c17	n5‐c17	VERB
eurjchem-228	199	54	1.453	1.453	NUM
eurjchem-228	199	55	(	(	PUNCT
eurjchem-228	199	56	6	6	NUM
eurjchem-228	199	57	)	)	PUNCT
eurjchem-228	199	58	n2‐c15‐c9	n2‐c15‐c9	PROPN
eurjchem-228	199	59	114.7	114.7	NUM
eurjchem-228	199	60	(	(	PUNCT
eurjchem-228	199	61	3	3	NUM
eurjchem-228	199	62	)	)	PUNCT
eurjchem-228	199	63	c7‐c15	c7‐c15	VERB
eurjchem-228	199	64	1.349	1.349	NUM
eurjchem-228	199	65	(	(	PUNCT
eurjchem-228	199	66	5	5	NUM
eurjchem-228	199	67	)	)	PUNCT
eurjchem-228	199	68	n2‐c15‐c7	n2‐c15‐c7	ADP
eurjchem-228	199	69	123.5	123.5	NUM
eurjchem-228	199	70	(	(	PUNCT
eurjchem-228	199	71	3	3	NUM
eurjchem-228	199	72	)	)	PUNCT
eurjchem-228	199	73	n5‐c18	n5‐c18	ADP
eurjchem-228	199	74	1.448	1.448	NUM
eurjchem-228	199	75	(	(	PUNCT
eurjchem-228	199	76	6	6	NUM
eurjchem-228	199	77	)	)	PUNCT
eurjchem-228	199	78	n5‐c7‐h7	n5‐c7‐h7	PROPN
eurjchem-228	199	79	120.3	120.3	NUM
eurjchem-228	199	80	(	(	PUNCT
eurjchem-228	199	81	4	4	NUM
eurjchem-228	199	82	)	)	PUNCT
eurjchem-228	199	83	n5‐c7‐c15‐c9	n5‐c7‐c15‐c9	PROPN
eurjchem-228	200	1	‐179.4	‐179.4	PROPN
eurjchem-228	200	2	(	(	PUNCT
eurjchem-228	200	3	7	7	NUM
eurjchem-228	200	4	)	)	PUNCT
eurjchem-228	200	5	scheme	scheme	NOUN
eurjchem-228	200	6	1	1	NUM
eurjchem-228	200	7	compound	compound	NOUN
eurjchem-228	200	8	2b	2b	NOUN
eurjchem-228	200	9	undergoes	undergo	VERB
eurjchem-228	200	10	self‐condensation	self‐condensation	NOUN
eurjchem-228	200	11	on	on	ADP
eurjchem-228	200	12	heating	heating	NOUN
eurjchem-228	200	13	in	in	ADP
eurjchem-228	200	14	focused	focused	ADJ
eurjchem-228	200	15	microwave	microwave	NOUN
eurjchem-228	200	16	at	at	ADP
eurjchem-228	200	17	140	140	NUM
eurjchem-228	200	18	oc	oc	NOUN
eurjchem-228	200	19	for	for	ADP
eurjchem-228	200	20	30	30	NUM
eurjchem-228	200	21	min	min	NOUN
eurjchem-228	200	22	in	in	ADP
eurjchem-228	200	23	presence	presence	NOUN
eurjchem-228	200	24	of	of	ADP
eurjchem-228	200	25	a	a	DET
eurjchem-228	200	26	few	few	ADJ
eurjchem-228	200	27	drops	drop	NOUN
eurjchem-228	200	28	of	of	ADP
eurjchem-228	200	29	acetic	acetic	ADJ
eurjchem-228	200	30	acid	acid	NOUN
eurjchem-228	200	31	to	to	PART
eurjchem-228	200	32	give	give	VERB
eurjchem-228	200	33	1,3,5‐triacylbenzene	1,3,5‐triacylbenzene	NUM
eurjchem-228	200	34	6b	6b	NOUN
eurjchem-228	200	35	in	in	ADP
eurjchem-228	200	36	93	93	NUM
eurjchem-228	200	37	%	%	NOUN
eurjchem-228	200	38	yields	yield	NOUN
eurjchem-228	200	39	.	.	PUNCT
eurjchem-228	201	1	we	we	PRON
eurjchem-228	201	2	believe	believe	VERB
eurjchem-228	201	3	that	that	SCONJ
eurjchem-228	201	4	compound	compound	NOUN
eurjchem-228	201	5	2b	2b	NOUN
eurjchem-228	201	6	is	be	AUX
eurjchem-228	201	7	initially	initially	ADV
eurjchem-228	201	8	converted	convert	VERB
eurjchem-228	201	9	to	to	ADP
eurjchem-228	201	10	the	the	DET
eurjchem-228	201	11	open	open	ADJ
eurjchem-228	201	12	chain	chain	NOUN
eurjchem-228	201	13	intermediate	intermediate	ADJ
eurjchem-228	201	14	4	4	NUM
eurjchem-228	201	15	that	that	PRON
eurjchem-228	201	16	further	far	ADV
eurjchem-228	201	17	adds	add	VERB
eurjchem-228	201	18	to	to	ADP
eurjchem-228	201	19	one	one	NUM
eurjchem-228	201	20	molecule	molecule	NOUN
eurjchem-228	201	21	of	of	ADP
eurjchem-228	201	22	enaminone	enaminone	NOUN
eurjchem-228	201	23	2b	2b	NOUN
eurjchem-228	201	24	to	to	PART
eurjchem-228	201	25	yield	yield	VERB
eurjchem-228	201	26	the	the	DET
eurjchem-228	201	27	intermediate	intermediate	ADJ
eurjchem-228	201	28	5	5	NUM
eurjchem-228	201	29	,	,	PUNCT
eurjchem-228	201	30	which	which	PRON
eurjchem-228	201	31	aromatize	aromatize	VERB
eurjchem-228	201	32	under	under	ADP
eurjchem-228	201	33	these	these	DET
eurjchem-228	201	34	reaction	reaction	NOUN
eurjchem-228	201	35	conditions	condition	NOUN
eurjchem-228	201	36	to	to	PART
eurjchem-228	201	37	give	give	VERB
eurjchem-228	201	38	the	the	DET
eurjchem-228	201	39	final	final	ADJ
eurjchem-228	201	40	isolable	isolable	ADJ
eurjchem-228	201	41	product	product	NOUN
eurjchem-228	201	42	6b	6b	NOUN
eurjchem-228	201	43	.	.	PUNCT
eurjchem-228	202	1	in	in	ADP
eurjchem-228	202	2	a	a	DET
eurjchem-228	202	3	trial	trial	NOUN
eurjchem-228	202	4	to	to	PART
eurjchem-228	202	5	enhance	enhance	VERB
eurjchem-228	202	6	the	the	DET
eurjchem-228	202	7	polycondensation	polycondensation	NOUN
eurjchem-228	202	8	of	of	ADP
eurjchem-228	202	9	2a	2a	NUM
eurjchem-228	202	10	using	use	VERB
eurjchem-228	202	11	incl3	incl3	PROPN
eurjchem-228	202	12	as	as	ADP
eurjchem-228	202	13	catalyst	catalyst	NOUN
eurjchem-228	202	14	the	the	DET
eurjchem-228	202	15	reaction	reaction	NOUN
eurjchem-228	202	16	resulted	result	VERB
eurjchem-228	202	17	only	only	ADV
eurjchem-228	202	18	in	in	ADP
eurjchem-228	202	19	the	the	DET
eurjchem-228	202	20	formation	formation	NOUN
eurjchem-228	202	21	of	of	ADP
eurjchem-228	202	22	6a	6a	NOUN
eurjchem-228	202	23	,	,	PUNCT
eurjchem-228	202	24	which	which	PRON
eurjchem-228	202	25	has	have	AUX
eurjchem-228	202	26	been	be	AUX
eurjchem-228	202	27	recently	recently	ADV
eurjchem-228	202	28	reported	report	VERB
eurjchem-228	202	29	by	by	ADP
eurjchem-228	202	30	us	we	PRON
eurjchem-228	202	31	[	[	X
eurjchem-228	202	32	16	16	NUM
eurjchem-228	202	33	]	]	PUNCT
eurjchem-228	202	34	(	(	PUNCT
eurjchem-228	202	35	scheme	scheme	NOUN
eurjchem-228	202	36	2	2	NUM
eurjchem-228	202	37	)	)	PUNCT
eurjchem-228	202	38	.	.	PUNCT
eurjchem-228	203	1	compounds	compound	VERB
eurjchem-228	203	2	2a‐c	2a‐c	PROPN
eurjchem-228	203	3	,	,	PUNCT
eurjchem-228	203	4	have	have	AUX
eurjchem-228	203	5	proved	prove	VERB
eurjchem-228	203	6	to	to	PART
eurjchem-228	203	7	be	be	AUX
eurjchem-228	203	8	a	a	DET
eurjchem-228	203	9	versatile	versatile	ADJ
eurjchem-228	203	10	starting	starting	NOUN
eurjchem-228	203	11	materials	material	NOUN
eurjchem-228	203	12	for	for	ADP
eurjchem-228	203	13	a	a	DET
eurjchem-228	203	14	variety	variety	NOUN
eurjchem-228	203	15	of	of	ADP
eurjchem-228	203	16	otherwise	otherwise	ADV
eurjchem-228	203	17	not	not	PART
eurjchem-228	203	18	readily	readily	ADV
eurjchem-228	203	19	obtainable	obtainable	ADJ
eurjchem-228	203	20	functionally	functionally	ADV
eurjchem-228	203	21	substituted	substitute	VERB
eurjchem-228	203	22	aromatics	aromatic	NOUN
eurjchem-228	203	23	and	and	CCONJ
eurjchem-228	203	24	heteroaromatics	heteroaromatic	NOUN
eurjchem-228	203	25	.	.	PUNCT
eurjchem-228	204	1	thus	thus	ADV
eurjchem-228	204	2	,	,	PUNCT
eurjchem-228	204	3	heating	heat	VERB
eurjchem-228	204	4	a	a	DET
eurjchem-228	204	5	mixture	mixture	NOUN
eurjchem-228	204	6	of	of	ADP
eurjchem-228	204	7	enaminones	enaminone	NOUN
eurjchem-228	204	8	2a	2a	NUM
eurjchem-228	204	9	with	with	ADP
eurjchem-228	204	10	2b	2b	NUM
eurjchem-228	204	11	or	or	CCONJ
eurjchem-228	204	12	2c	2c	NOUN
eurjchem-228	204	13	as	as	ADP
eurjchem-228	204	14	2:1	2:1	NUM
eurjchem-228	204	15	ratio	ratio	NOUN
eurjchem-228	204	16	in	in	ADP
eurjchem-228	204	17	focused	focused	ADJ
eurjchem-228	204	18	microwave	microwave	NOUN
eurjchem-228	204	19	oven	oven	NOUN
eurjchem-228	204	20	at	at	ADP
eurjchem-228	204	21	140	140	NUM
eurjchem-228	204	22	°	°	ADP
eurjchem-228	204	23	c	c	NOUN
eurjchem-228	204	24	for	for	ADP
eurjchem-228	204	25	30	30	NUM
eurjchem-228	204	26	min	min	NOUN
eurjchem-228	204	27	in	in	ADP
eurjchem-228	204	28	presence	presence	NOUN
eurjchem-228	204	29	of	of	ADP
eurjchem-228	204	30	few	few	ADJ
eurjchem-228	204	31	drops	drop	NOUN
eurjchem-228	204	32	of	of	ADP
eurjchem-228	204	33	acetic	acetic	ADJ
eurjchem-228	204	34	acid	acid	NOUN
eurjchem-228	204	35	afforded	afford	VERB
eurjchem-228	204	36	products	product	NOUN
eurjchem-228	204	37	that	that	PRON
eurjchem-228	204	38	were	be	AUX
eurjchem-228	204	39	identified	identify	VERB
eurjchem-228	204	40	as	as	ADP
eurjchem-228	204	41	1,3,5‐trisubstituted	1,3,5‐trisubstituted	NUM
eurjchem-228	204	42	benzenes	benzene	NOUN
eurjchem-228	204	43	8a	8a	NUM
eurjchem-228	204	44	,	,	PUNCT
eurjchem-228	204	45	b	b	NOUN
eurjchem-228	204	46	in	in	ADP
eurjchem-228	204	47	52	52	NUM
eurjchem-228	204	48	%	%	NOUN
eurjchem-228	204	49	and	and	CCONJ
eurjchem-228	204	50	68	68	NUM
eurjchem-228	204	51	%	%	NOUN
eurjchem-228	204	52	yields	yield	NOUN
eurjchem-228	204	53	,	,	PUNCT
eurjchem-228	204	54	respectively	respectively	ADV
eurjchem-228	204	55	.	.	PUNCT
eurjchem-228	205	1	it	it	PRON
eurjchem-228	205	2	is	be	AUX
eurjchem-228	205	3	most	most	ADV
eurjchem-228	205	4	likely	likely	ADJ
eurjchem-228	205	5	that	that	SCONJ
eurjchem-228	205	6	the	the	DET
eurjchem-228	205	7	initial	initial	ADJ
eurjchem-228	205	8	step	step	NOUN
eurjchem-228	205	9	in	in	ADP
eurjchem-228	205	10	this	this	DET
eurjchem-228	205	11	reaction	reaction	NOUN
eurjchem-228	205	12	is	be	AUX
eurjchem-228	205	13	addition	addition	NOUN
eurjchem-228	205	14	of	of	ADP
eurjchem-228	205	15	2a	2a	NUM
eurjchem-228	205	16	to	to	ADP
eurjchem-228	205	17	2b	2b	NUM
eurjchem-228	205	18	or	or	CCONJ
eurjchem-228	205	19	2c	2c	NUM
eurjchem-228	205	20	to	to	PART
eurjchem-228	205	21	furnish	furnish	VERB
eurjchem-228	205	22	an	an	DET
eurjchem-228	205	23	intermediate	intermediate	ADJ
eurjchem-228	205	24	7	7	NUM
eurjchem-228	205	25	,	,	PUNCT
eurjchem-228	205	26	which	which	PRON
eurjchem-228	205	27	then	then	ADV
eurjchem-228	205	28	reacts	react	VERB
eurjchem-228	205	29	further	far	ADV
eurjchem-228	205	30	with	with	ADP
eurjchem-228	205	31	2a	2a	NUM
eurjchem-228	205	32	to	to	PART
eurjchem-228	205	33	yield	yield	VERB
eurjchem-228	205	34	final	final	ADJ
eurjchem-228	205	35	isolable	isolable	ADJ
eurjchem-228	205	36	products	product	NOUN
eurjchem-228	205	37	8a	8a	NUM
eurjchem-228	205	38	,	,	PUNCT
eurjchem-228	205	39	b	b	PROPN
eurjchem-228	205	40	(	(	PUNCT
eurjchem-228	205	41	scheme	scheme	NOUN
eurjchem-228	205	42	3	3	NUM
eurjchem-228	205	43	)	)	PUNCT
eurjchem-228	205	44	.	.	PUNCT
eurjchem-228	206	1	el‐apasery	el‐apasery	NOUN
eurjchem-228	206	2	et	et	PROPN
eurjchem-228	206	3	al	al	PROPN
eurjchem-228	206	4	.	.	PUNCT
eurjchem-228	206	5	/	/	SYM
eurjchem-228	206	6	european	european	PROPN
eurjchem-228	206	7	journal	journal	PROPN
eurjchem-228	206	8	of	of	ADP
eurjchem-228	206	9	chemistry	chemistry	NOUN
eurjchem-228	206	10	2	2	NUM
eurjchem-228	206	11	(	(	PUNCT
eurjchem-228	206	12	2	2	NUM
eurjchem-228	206	13	)	)	PUNCT
eurjchem-228	206	14	(	(	PUNCT
eurjchem-228	206	15	2011	2011	NUM
eurjchem-228	206	16	)	)	PUNCT
eurjchem-228	206	17	168‐172	168‐172	NUM
eurjchem-228	206	18	171	171	NUM
eurjchem-228	206	19	scheme	scheme	NOUN
eurjchem-228	206	20	2	2	NUM
eurjchem-228	206	21	scheme	scheme	NOUN
eurjchem-228	206	22	3	3	NUM
eurjchem-228	206	23	compound	compound	NOUN
eurjchem-228	206	24	2a‐c	2a‐c	NOUN
eurjchem-228	206	25	reacted	react	VERB
eurjchem-228	206	26	with	with	ADP
eurjchem-228	206	27	aniline	aniline	NOUN
eurjchem-228	206	28	in	in	ADP
eurjchem-228	206	29	focused	focused	ADJ
eurjchem-228	206	30	microwave	microwave	NOUN
eurjchem-228	206	31	oven	oven	NOUN
eurjchem-228	206	32	at	at	ADP
eurjchem-228	206	33	140	140	NUM
eurjchem-228	206	34	ºc	ºc	NOUN
eurjchem-228	206	35	for	for	ADP
eurjchem-228	206	36	5	5	NUM
eurjchem-228	206	37	min	min	NOUN
eurjchem-228	206	38	afforded	afford	VERB
eurjchem-228	206	39	the	the	DET
eurjchem-228	206	40	aniline	aniline	ADJ
eurjchem-228	206	41	derivatives	derivative	NOUN
eurjchem-228	206	42	9a‐c	9a‐c	NOUN
eurjchem-228	206	43	in	in	ADP
eurjchem-228	206	44	88	88	NUM
eurjchem-228	206	45	%	%	NOUN
eurjchem-228	206	46	,	,	PUNCT
eurjchem-228	206	47	74	74	NUM
eurjchem-228	206	48	%	%	NOUN
eurjchem-228	206	49	and	and	CCONJ
eurjchem-228	206	50	83	83	NUM
eurjchem-228	206	51	%	%	NOUN
eurjchem-228	206	52	yields	yield	NOUN
eurjchem-228	206	53	,	,	PUNCT
eurjchem-228	206	54	respectively	respectively	ADV
eurjchem-228	206	55	(	(	PUNCT
eurjchem-228	206	56	scheme	scheme	NOUN
eurjchem-228	206	57	4	4	NUM
eurjchem-228	206	58	)	)	PUNCT
eurjchem-228	206	59	.	.	PUNCT
eurjchem-228	207	1	heating	heating	NOUN
eurjchem-228	207	2	enaminones	enaminone	NOUN
eurjchem-228	207	3	2a	2a	NUM
eurjchem-228	207	4	,	,	PUNCT
eurjchem-228	207	5	b	b	NOUN
eurjchem-228	207	6	with	with	ADP
eurjchem-228	207	7	ammonium	ammonium	NOUN
eurjchem-228	207	8	acetate	acetate	NOUN
eurjchem-228	207	9	,	,	PUNCT
eurjchem-228	207	10	in	in	ADP
eurjchem-228	207	11	focused	focused	ADJ
eurjchem-228	207	12	microwave	microwave	NOUN
eurjchem-228	207	13	oven	oven	NOUN
eurjchem-228	207	14	at	at	ADP
eurjchem-228	207	15	160‐140	160‐140	NUM
eurjchem-228	207	16	oc	oc	NOUN
eurjchem-228	207	17	for	for	ADP
eurjchem-228	207	18	10	10	NUM
eurjchem-228	207	19	min	min	NOUN
eurjchem-228	207	20	afforded	afford	VERB
eurjchem-228	207	21	the	the	DET
eurjchem-228	207	22	3‐aroyl‐6‐substituted	3‐aroyl‐6‐substituted	ADJ
eurjchem-228	207	23	pyridines	pyridine	NOUN
eurjchem-228	207	24	12a	12a	NOUN
eurjchem-228	207	25	,	,	PUNCT
eurjchem-228	207	26	b	b	NOUN
eurjchem-228	207	27	in	in	ADP
eurjchem-228	207	28	53	53	NUM
eurjchem-228	207	29	%	%	NOUN
eurjchem-228	207	30	and	and	CCONJ
eurjchem-228	207	31	78	78	NUM
eurjchem-228	207	32	%	%	NOUN
eurjchem-228	207	33	yields	yield	NOUN
eurjchem-228	207	34	,	,	PUNCT
eurjchem-228	207	35	respectively	respectively	ADV
eurjchem-228	207	36	.	.	PUNCT
eurjchem-228	208	1	formation	formation	NOUN
eurjchem-228	208	2	of	of	ADP
eurjchem-228	208	3	12a	12a	NOUN
eurjchem-228	208	4	,	,	PUNCT
eurjchem-228	208	5	b	b	NOUN
eurjchem-228	208	6	may	may	AUX
eurjchem-228	208	7	take	take	VERB
eurjchem-228	208	8	place	place	NOUN
eurjchem-228	208	9	through	through	ADP
eurjchem-228	208	10	an	an	DET
eurjchem-228	208	11	initial	initial	ADJ
eurjchem-228	208	12	self	self	NOUN
eurjchem-228	208	13	condensation	condensation	NOUN
eurjchem-228	208	14	of	of	ADP
eurjchem-228	208	15	2	2	NUM
eurjchem-228	208	16	to	to	PART
eurjchem-228	208	17	afford	afford	VERB
eurjchem-228	208	18	the	the	DET
eurjchem-228	208	19	intermediate	intermediate	ADJ
eurjchem-228	208	20	10	10	NUM
eurjchem-228	208	21	which	which	PRON
eurjchem-228	208	22	reacts	react	VERB
eurjchem-228	208	23	directly	directly	ADV
eurjchem-228	208	24	with	with	ADP
eurjchem-228	208	25	ammonium	ammonium	NOUN
eurjchem-228	208	26	ion	ion	NOUN
eurjchem-228	208	27	to	to	PART
eurjchem-228	208	28	give	give	VERB
eurjchem-228	208	29	a	a	DET
eurjchem-228	208	30	further	further	ADJ
eurjchem-228	208	31	intermediate	intermediate	ADJ
eurjchem-228	208	32	11	11	NUM
eurjchem-228	208	33	,	,	PUNCT
eurjchem-228	208	34	that	that	PRON
eurjchem-228	208	35	undergoes	undergo	VERB
eurjchem-228	208	36	intramolecular	intramolecular	ADJ
eurjchem-228	208	37	cycloconden‐	cycloconden‐	NOUN
eurjchem-228	208	38	sation	sation	NOUN
eurjchem-228	208	39	,	,	PUNCT
eurjchem-228	208	40	via	via	ADP
eurjchem-228	208	41	loss	loss	NOUN
eurjchem-228	208	42	one	one	NUM
eurjchem-228	208	43	molecule	molecule	NOUN
eurjchem-228	208	44	of	of	ADP
eurjchem-228	208	45	water	water	NOUN
eurjchem-228	208	46	to	to	PART
eurjchem-228	208	47	give	give	VERB
eurjchem-228	208	48	the	the	DET
eurjchem-228	208	49	final	final	ADJ
eurjchem-228	208	50	products	product	NOUN
eurjchem-228	208	51	(	(	PUNCT
eurjchem-228	208	52	scheme	scheme	NOUN
eurjchem-228	208	53	5	5	NUM
eurjchem-228	208	54	)	)	PUNCT
eurjchem-228	208	55	.	.	PUNCT
eurjchem-228	209	1	4	4	X
eurjchem-228	209	2	.	.	X
eurjchem-228	209	3	conclusion	conclusion	NOUN
eurjchem-228	209	4	the	the	DET
eurjchem-228	209	5	studies	study	NOUN
eurjchem-228	209	6	described	describe	VERB
eurjchem-228	209	7	above	above	ADP
eurjchem-228	209	8	clearly	clearly	ADV
eurjchem-228	209	9	demonstrate	demonstrate	VERB
eurjchem-228	209	10	that	that	SCONJ
eurjchem-228	209	11	an	an	DET
eurjchem-228	209	12	efficient	efficient	ADJ
eurjchem-228	209	13	method	method	NOUN
eurjchem-228	209	14	was	be	AUX
eurjchem-228	209	15	achieved	achieve	VERB
eurjchem-228	209	16	for	for	ADP
eurjchem-228	209	17	the	the	DET
eurjchem-228	209	18	preparation	preparation	NOUN
eurjchem-228	209	19	of	of	ADP
eurjchem-228	209	20	enaminones	enaminone	NOUN
eurjchem-228	209	21	,	,	PUNCT
eurjchem-228	209	22	employing	employ	VERB
eurjchem-228	209	23	green	green	ADJ
eurjchem-228	209	24	methodologies	methodology	NOUN
eurjchem-228	209	25	.	.	PUNCT
eurjchem-228	210	1	the	the	DET
eurjchem-228	210	2	simplicity	simplicity	NOUN
eurjchem-228	210	3	of	of	ADP
eurjchem-228	210	4	the	the	DET
eurjchem-228	210	5	reaction	reaction	NOUN
eurjchem-228	210	6	conditions	condition	NOUN
eurjchem-228	210	7	,	,	PUNCT
eurjchem-228	210	8	their	their	PRON
eurjchem-228	210	9	efficacy	efficacy	NOUN
eurjchem-228	210	10	and	and	CCONJ
eurjchem-228	210	11	excellent	excellent	ADJ
eurjchem-228	210	12	yields	yield	NOUN
eurjchem-228	210	13	obtained	obtain	VERB
eurjchem-228	210	14	using	use	VERB
eurjchem-228	210	15	mw	mw	NOUN
eurjchem-228	210	16	irradiation	irradiation	NOUN
eurjchem-228	210	17	,	,	PUNCT
eurjchem-228	210	18	under	under	ADP
eurjchem-228	210	19	solvent‐	solvent‐	PROPN
eurjchem-228	210	20	and	and	CCONJ
eurjchem-228	210	21	catalyst‐free	catalyst‐free	ADJ
eurjchem-228	210	22	conditions	condition	NOUN
eurjchem-228	210	23	.	.	PUNCT
eurjchem-228	211	1	also	also	ADV
eurjchem-228	211	2	we	we	PRON
eurjchem-228	211	3	could	could	AUX
eurjchem-228	211	4	show	show	VERB
eurjchem-228	211	5	that	that	SCONJ
eurjchem-228	211	6	the	the	DET
eurjchem-228	211	7	enaminones	enaminone	NOUN
eurjchem-228	211	8	2a‐c	2a‐c	NOUN
eurjchem-228	211	9	is	be	AUX
eurjchem-228	211	10	a	a	DET
eurjchem-228	211	11	valuable	valuable	ADJ
eurjchem-228	211	12	precursor	precursor	NOUN
eurjchem-228	211	13	to	to	ADP
eurjchem-228	211	14	the	the	DET
eurjchem-228	211	15	triacylbenzene	triacylbenzene	ADJ
eurjchem-228	211	16	1,3,5‐trisubstituted	1,3,5‐trisubstituted	NUM
eurjchem-228	211	17	benzenes	benzene	NOUN
eurjchem-228	211	18	as	as	ADV
eurjchem-228	211	19	well	well	ADV
eurjchem-228	211	20	as	as	ADP
eurjchem-228	211	21	3‐aroyl‐6‐substituted	3‐aroyl‐6‐substituted	NUM
eurjchem-228	211	22	pyridines	pyridine	NOUN
eurjchem-228	211	23	.	.	PUNCT
eurjchem-228	212	1	scheme	scheme	NOUN
eurjchem-228	212	2	4	4	NUM
eurjchem-228	212	3	scheme	scheme	NOUN
eurjchem-228	212	4	5	5	NUM
eurjchem-228	212	5	acknowledgements	acknowledgement	NOUN
eurjchem-228	212	6	financial	financial	ADJ
eurjchem-228	212	7	support	support	NOUN
eurjchem-228	212	8	of	of	ADP
eurjchem-228	212	9	this	this	DET
eurjchem-228	212	10	work	work	NOUN
eurjchem-228	212	11	from	from	ADP
eurjchem-228	212	12	kuwait	kuwait	PROPN
eurjchem-228	212	13	university	university	PROPN
eurjchem-228	212	14	research	research	NOUN
eurjchem-228	212	15	fund	fund	NOUN
eurjchem-228	212	16	(	(	PUNCT
eurjchem-228	212	17	projects	project	VERB
eurjchem-228	212	18	no	no	NOUN
eurjchem-228	212	19	:	:	PUNCT
eurjchem-228	212	20	sc05/09	sc05/09	NOUN
eurjchem-228	212	21	)	)	PUNCT
eurjchem-228	212	22	and	and	CCONJ
eurjchem-228	212	23	by	by	ADP
eurjchem-228	212	24	a	a	DET
eurjchem-228	212	25	research	research	NOUN
eurjchem-228	212	26	grant	grant	NOUN
eurjchem-228	212	27	from	from	ADP
eurjchem-228	212	28	analab./saf	analab./saf	PROPN
eurjchem-228	212	29	(	(	PUNCT
eurjchem-228	212	30	gc01/03	gc01/03	PROPN
eurjchem-228	212	31	,	,	PUNCT
eurjchem-228	212	32	gc01/05	gc01/05	NOUN
eurjchem-228	212	33	and	and	CCONJ
eurjchem-228	212	34	gs03/01	gs03/01	NOUN
eurjchem-228	212	35	)	)	PUNCT
eurjchem-228	212	36	is	be	AUX
eurjchem-228	212	37	gratefully	gratefully	ADV
eurjchem-228	212	38	acknowledged	acknowledge	VERB
eurjchem-228	212	39	..	..	PUNCT
eurjchem-228	212	40	supplementary	supplementary	ADJ
eurjchem-228	212	41	material	material	NOUN
eurjchem-228	212	42	ccdc‐772198	ccdc‐772198	PROPN
eurjchem-228	212	43	contains	contain	VERB
eurjchem-228	212	44	the	the	DET
eurjchem-228	212	45	supplementary	supplementary	ADJ
eurjchem-228	212	46	crystallographic	crystallographic	ADJ
eurjchem-228	212	47	data	datum	NOUN
eurjchem-228	212	48	for	for	ADP
eurjchem-228	212	49	this	this	DET
eurjchem-228	212	50	paper	paper	NOUN
eurjchem-228	212	51	.	.	PUNCT
eurjchem-228	213	1	these	these	DET
eurjchem-228	213	2	data	datum	NOUN
eurjchem-228	213	3	can	can	AUX
eurjchem-228	213	4	be	be	AUX
eurjchem-228	213	5	obtained	obtain	VERB
eurjchem-228	213	6	free	free	ADJ
eurjchem-228	213	7	of	of	ADP
eurjchem-228	213	8	charge	charge	NOUN
eurjchem-228	213	9	via	via	ADP
eurjchem-228	213	10	www.ccdc.cam.ac.uk/data_request/cif	www.ccdc.cam.ac.uk/data_request/cif	NOUN
eurjchem-228	213	11	,	,	PUNCT
eurjchem-228	213	12	or	or	CCONJ
eurjchem-228	213	13	by	by	ADP
eurjchem-228	213	14	e‐mailing	e‐maile	VERB
eurjchem-228	213	15	data_request@ccdc.cam.ac.uk	data_request@ccdc.cam.ac.uk	VERB
eurjchem-228	213	16	,	,	PUNCT
eurjchem-228	213	17	or	or	CCONJ
eurjchem-228	213	18	by	by	ADP
eurjchem-228	213	19	contacting	contact	VERB
eurjchem-228	213	20	the	the	DET
eurjchem-228	213	21	cambridge	cambridge	PROPN
eurjchem-228	213	22	crystallographic	crystallographic	PROPN
eurjchem-228	213	23	data	data	PROPN
eurjchem-228	213	24	centre	centre	NOUN
eurjchem-228	213	25	,	,	PUNCT
eurjchem-228	213	26	12	12	NUM
eurjchem-228	213	27	union	union	NOUN
eurjchem-228	213	28	road	road	NOUN
eurjchem-228	213	29	,	,	PUNCT
eurjchem-228	213	30	cambridge	cambridge	PROPN
eurjchem-228	213	31	cb2	cb2	PROPN
eurjchem-228	213	32	1ez	1ez	PROPN
eurjchem-228	213	33	,	,	PUNCT
eurjchem-228	213	34	uk	uk	PROPN
eurjchem-228	213	35	;	;	PUNCT
eurjchem-228	213	36	fax	fax	NOUN
eurjchem-228	213	37	:	:	PUNCT
eurjchem-228	213	38	+44(0)1223‐336033	+44(0)1223‐336033	ADJ
eurjchem-228	213	39	.	.	PUNCT
eurjchem-228	213	40	references	reference	NOUN
eurjchem-228	213	41	[	[	X
eurjchem-228	213	42	1	1	NUM
eurjchem-228	213	43	]	]	PUNCT
eurjchem-228	213	44	.	.	PUNCT
eurjchem-228	214	1	zhu	zhu	PROPN
eurjchem-228	214	2	,	,	PUNCT
eurjchem-228	214	3	s.	s.	PROPN
eurjchem-228	214	4	;	;	PUNCT
eurjchem-228	214	5	zhao	zhao	PROPN
eurjchem-228	214	6	,	,	PUNCT
eurjchem-228	214	7	k.	k.	PROPN
eurjchem-228	214	8	;	;	PUNCT
eurjchem-228	214	9	su	su	PROPN
eurjchem-228	214	10	,	,	PUNCT
eurjchem-228	214	11	x.	x.	PROPN
eurjchem-228	214	12	;	;	PUNCT
eurjchem-228	214	13	ji	ji	PROPN
eurjchem-228	214	14	,	,	PUNCT
eurjchem-228	214	15	s.	s.	PROPN
eurjchem-228	214	16	synth	synth	PROPN
eurjchem-228	214	17	.	.	PUNCT
eurjchem-228	215	1	commun	commun	PROPN
eurjchem-228	215	2	.	.	PUNCT
eurjchem-228	216	1	2009	2009	NUM
eurjchem-228	216	2	,	,	PUNCT
eurjchem-228	216	3	39	39	NUM
eurjchem-228	216	4	,	,	PUNCT
eurjchem-228	216	5	1355‐1366	1355‐1366	NUM
eurjchem-228	216	6	.	.	PUNCT
eurjchem-228	217	1	[	[	X
eurjchem-228	217	2	2	2	NUM
eurjchem-228	217	3	]	]	PUNCT
eurjchem-228	217	4	.	.	PUNCT
eurjchem-228	218	1	loghmani‐khouzani	loghmani‐khouzani	PROPN
eurjchem-228	218	2	,	,	PUNCT
eurjchem-228	218	3	h.	h.	PROPN
eurjchem-228	218	4	;	;	PUNCT
eurjchem-228	218	5	sabzyan	sabzyan	PROPN
eurjchem-228	218	6	,	,	PUNCT
eurjchem-228	218	7	h	h	NOUN
eurjchem-228	218	8	;	;	PUNCT
eurjchem-228	218	9	rezaei‐pooranari	rezaei‐pooranari	PROPN
eurjchem-228	218	10	,	,	PUNCT
eurjchem-228	218	11	a.	a.	NOUN
eurjchem-228	218	12	dyes	dye	NOUN
eurjchem-228	218	13	pigments	pigment	NOUN
eurjchem-228	218	14	2008	2008	NUM
eurjchem-228	218	15	,	,	PUNCT
eurjchem-228	218	16	76	76	NUM
eurjchem-228	218	17	,	,	PUNCT
eurjchem-228	218	18	447‐454	447‐454	PROPN
eurjchem-228	218	19	.	.	PUNCT
eurjchem-228	219	1	172	172	NUM
eurjchem-228	219	2	el‐apasery	el‐apasery	PROPN
eurjchem-228	219	3	et	et	PROPN
eurjchem-228	219	4	al	al	PROPN
eurjchem-228	219	5	.	.	PUNCT
eurjchem-228	219	6	/	/	SYM
eurjchem-228	219	7	european	european	PROPN
eurjchem-228	219	8	journal	journal	PROPN
eurjchem-228	219	9	of	of	ADP
eurjchem-228	219	10	chemistry	chemistry	NOUN
eurjchem-228	219	11	2	2	NUM
eurjchem-228	219	12	(	(	PUNCT
eurjchem-228	219	13	2	2	NUM
eurjchem-228	219	14	)	)	PUNCT
eurjchem-228	219	15	(	(	PUNCT
eurjchem-228	219	16	2011	2011	NUM
eurjchem-228	219	17	)	)	PUNCT
eurjchem-228	219	18	168‐172	168‐172	NUM
eurjchem-228	220	1	[	[	X
eurjchem-228	220	2	3	3	NUM
eurjchem-228	220	3	]	]	PUNCT
eurjchem-228	220	4	.	.	PUNCT
eurjchem-228	221	1	riyadh	riyadh	PROPN
eurjchem-228	221	2	,	,	PUNCT
eurjchem-228	221	3	s.	s.	PROPN
eurjchem-228	221	4	m.	m.	PROPN
eurjchem-228	221	5	;	;	PUNCT
eurjchem-228	221	6	abdelhamid	abdelhamid	PROPN
eurjchem-228	221	7	,	,	PUNCT
eurjchem-228	221	8	i.	i.	PROPN
eurjchem-228	221	9	a.	a.	PROPN
eurjchem-228	221	10	;	;	PUNCT
eurjchem-228	221	11	al‐matar	al‐matar	PROPN
eurjchem-228	221	12	,	,	PUNCT
eurjchem-228	221	13	h.	h.	PROPN
eurjchem-228	221	14	m.	m.	NOUN
eurjchem-228	221	15	;	;	PUNCT
eurjchem-228	221	16	hilmy	hilmy	INTJ
eurjchem-228	221	17	,	,	PUNCT
eurjchem-228	221	18	n.	n.	PROPN
eurjchem-228	221	19	h.	h.	PROPN
eurjchem-228	221	20	;	;	PUNCT
eurjchem-228	221	21	elnagdi	elnagdi	PROPN
eurjchem-228	221	22	,	,	PUNCT
eurjchem-228	221	23	m.	m.	NOUN
eurjchem-228	221	24	h.	h.	PROPN
eurjchem-228	221	25	heterocycles	heterocycles	PROPN
eurjchem-228	221	26	2008	2008	NUM
eurjchem-228	221	27	,	,	PUNCT
eurjchem-228	221	28	75	75	NUM
eurjchem-228	221	29	,	,	PUNCT
eurjchem-228	221	30	1849‐1905	1849‐1905	NUM
eurjchem-228	221	31	.	.	PUNCT
eurjchem-228	222	1	[	[	X
eurjchem-228	222	2	4	4	NUM
eurjchem-228	222	3	]	]	PUNCT
eurjchem-228	222	4	.	.	PUNCT
eurjchem-228	222	5	stanovnik	stanovnik	PROPN
eurjchem-228	222	6	,	,	PUNCT
eurjchem-228	222	7	b.	b.	PROPN
eurjchem-228	222	8	;	;	PUNCT
eurjchem-228	222	9	svete	svete	PROPN
eurjchem-228	222	10	,	,	PUNCT
eurjchem-228	222	11	j.	j.	PROPN
eurjchem-228	222	12	chem	chem	PROPN
eurjchem-228	222	13	.	.	PUNCT
eurjchem-228	223	1	rev	rev	PROPN
eurjchem-228	223	2	.	.	PROPN
eurjchem-228	223	3	2004	2004	NUM
eurjchem-228	223	4	,	,	PUNCT
eurjchem-228	223	5	104	104	NUM
eurjchem-228	223	6	,	,	PUNCT
eurjchem-228	223	7	2433‐2480	2433‐2480	NUM
eurjchem-228	223	8	.	.	PUNCT
eurjchem-228	224	1	[	[	X
eurjchem-228	224	2	5	5	NUM
eurjchem-228	224	3	]	]	PUNCT
eurjchem-228	224	4	.	.	PUNCT
eurjchem-228	225	1	sheikhshoaie	sheikhshoaie	PROPN
eurjchem-228	225	2	,	,	PUNCT
eurjchem-228	225	3	i.	i.	PROPN
eurjchem-228	225	4	f	f	PROPN
eurjchem-228	225	5	;	;	PUNCT
eurjchem-228	225	6	walter	walter	PROPN
eurjchem-228	225	7	m.	m.	PROPN
eurjchem-228	225	8	f.	f.	PROPN
eurjchem-228	225	9	curr	curr	PROPN
eurjchem-228	225	10	.	.	PUNCT
eurjchem-228	226	1	org	org	PROPN
eurjchem-228	226	2	.	.	PUNCT
eurjchem-228	226	3	chem	chem	PROPN
eurjchem-228	226	4	.	.	PUNCT
eurjchem-228	227	1	2009	2009	NUM
eurjchem-228	227	2	,	,	PUNCT
eurjchem-228	227	3	13(2	13(2	NOUN
eurjchem-228	227	4	)	)	PUNCT
eurjchem-228	227	5	,	,	PUNCT
eurjchem-228	227	6	149‐171	149‐171	NUM
eurjchem-228	227	7	.	.	PUNCT
eurjchem-228	228	1	[	[	X
eurjchem-228	228	2	6	6	NUM
eurjchem-228	228	3	]	]	PUNCT
eurjchem-228	228	4	.	.	PUNCT
eurjchem-228	229	1	macho	macho	ADJ
eurjchem-228	229	2	,	,	PUNCT
eurjchem-228	229	3	s.	s.	PROPN
eurjchem-228	229	4	;	;	PUNCT
eurjchem-228	229	5	miguel	miguel	PROPN
eurjchem-228	229	6	,	,	PUNCT
eurjchem-228	229	7	d.	d.	PROPN
eurjchem-228	229	8	;	;	PUNCT
eurjchem-228	229	9	neo	neo	PROPN
eurjchem-228	229	10	,	,	PUNCT
eurjchem-228	229	11	a.	a.	NOUN
eurjchem-228	229	12	g.	g.	PROPN
eurjchem-228	229	13	;	;	PUNCT
eurjchem-228	229	14	rodriguez	rodriguez	NOUN
eurjchem-228	229	15	,	,	PUNCT
eurjchem-228	229	16	t.	t.	PROPN
eurjchem-228	229	17	;	;	PUNCT
eurjchem-228	229	18	torroba	torroba	NOUN
eurjchem-228	229	19	,	,	PUNCT
eurjchem-228	229	20	t.	t.	NOUN
eurjchem-228	229	21	chem	chem	NOUN
eurjchem-228	229	22	.	.	PUNCT
eurjchem-228	230	1	commun	commun	PROPN
eurjchem-228	230	2	.	.	PUNCT
eurjchem-228	231	1	2005	2005	NUM
eurjchem-228	231	2	,	,	PUNCT
eurjchem-228	231	3	3	3	NUM
eurjchem-228	231	4	,	,	PUNCT
eurjchem-228	231	5	334‐336	334‐336	NUM
eurjchem-228	231	6	.	.	PUNCT
eurjchem-228	232	1	[	[	X
eurjchem-228	232	2	7	7	NUM
eurjchem-228	232	3	]	]	PUNCT
eurjchem-228	232	4	.	.	PUNCT
eurjchem-228	233	1	de	de	PROPN
eurjchem-228	233	2	oliveira	oliveira	PROPN
eurjchem-228	233	3	,	,	PUNCT
eurjchem-228	233	4	h.	h.	PROPN
eurjchem-228	233	5	c.	c.	PROPN
eurjchem-228	233	6	b.	b.	PROPN
eurjchem-228	233	7	;	;	PUNCT
eurjchem-228	233	8	fonseca	fonseca	PROPN
eurjchem-228	233	9	,	,	PUNCT
eurjchem-228	233	10	t.	t.	PROPN
eurjchem-228	233	11	l.	l.	PROPN
eurjchem-228	233	12	;	;	PUNCT
eurjchem-228	233	13	castro	castro	PROPN
eurjchem-228	233	14	,	,	PUNCT
eurjchem-228	233	15	m.	m.	NOUN
eurjchem-228	233	16	a.	a.	NOUN
eurjchem-228	233	17	;	;	PUNCT
eurjchem-228	233	18	amaral	amaral	PROPN
eurjchem-228	233	19	,	,	PUNCT
eurjchem-228	233	20	o.	o.	NOUN
eurjchem-228	233	21	a.	a.	NOUN
eurjchem-228	233	22	v.	v.	PROPN
eurjchem-228	233	23	;	;	PUNCT
eurjchem-228	233	24	cunha	cunha	NOUN
eurjchem-228	233	25	,	,	PUNCT
eurjchem-228	233	26	s.	s.	PROPN
eurjchem-228	233	27	j.	j.	PROPN
eurjchem-228	233	28	chem	chem	PROPN
eurjchem-228	233	29	.	.	PUNCT
eurjchem-228	234	1	phys	phy	NOUN
eurjchem-228	234	2	.	.	PUNCT
eurjchem-228	235	1	2003	2003	NUM
eurjchem-228	235	2	,	,	PUNCT
eurjchem-228	235	3	119(16	119(16	NUM
eurjchem-228	235	4	)	)	PUNCT
eurjchem-228	235	5	,	,	PUNCT
eurjchem-228	235	6	8417‐8424	8417‐8424	NUM
eurjchem-228	235	7	.	.	PUNCT
eurjchem-228	236	1	[	[	X
eurjchem-228	236	2	8	8	NUM
eurjchem-228	236	3	]	]	PUNCT
eurjchem-228	236	4	.	.	PUNCT
eurjchem-228	237	1	ghozlan	ghozlan	PROPN
eurjchem-228	237	2	s.	s.	PROPN
eurjchem-228	237	3	a.	a.	PROPN
eurjchem-228	237	4	s	s	PROPN
eurjchem-228	237	5	;	;	PUNCT
eurjchem-228	237	6	abdelhamid	abdelhamid	ADJ
eurjchem-228	237	7	,	,	PUNCT
eurjchem-228	237	8	i.	i.	PROPN
eurjchem-228	237	9	a.	a.	PROPN
eurjchem-228	237	10	;	;	PUNCT
eurjchem-228	237	11	gaber	gaber	PROPN
eurjchem-228	237	12	,	,	PUNCT
eurjchem-228	237	13	h.	h.	PROPN
eurjchem-228	237	14	;	;	PUNCT
eurjchem-228	237	15	elnagdi	elnagdi	PROPN
eurjchem-228	237	16	,	,	PUNCT
eurjchem-228	237	17	m.	m.	PROPN
eurjchem-228	237	18	h.	h.	PROPN
eurjchem-228	237	19	j.	j.	PROPN
eurjchem-228	237	20	heterocycl	heterocycl	PROPN
eurjchem-228	237	21	.	.	PUNCT
eurjchem-228	238	1	chem	chem	PROPN
eurjchem-228	238	2	.	.	PUNCT
eurjchem-228	239	1	2005	2005	NUM
eurjchem-228	239	2	,	,	PUNCT
eurjchem-228	239	3	42	42	NUM
eurjchem-228	239	4	,	,	PUNCT
eurjchem-228	239	5	1185‐1189	1185‐1189	NUM
eurjchem-228	239	6	.	.	PUNCT
eurjchem-228	240	1	[	[	X
eurjchem-228	240	2	9	9	NUM
eurjchem-228	240	3	]	]	PUNCT
eurjchem-228	240	4	.	.	PUNCT
eurjchem-228	241	1	al‐saleh	al‐saleh	NOUN
eurjchem-228	241	2	,	,	PUNCT
eurjchem-228	241	3	b.	b.	PROPN
eurjchem-228	241	4	;	;	PUNCT
eurjchem-228	241	5	makhseed	makhsee	VERB
eurjchem-228	241	6	,	,	PUNCT
eurjchem-228	241	7	s.	s.	PROPN
eurjchem-228	241	8	;	;	PUNCT
eurjchem-228	241	9	hassaneen	hassaneen	X
eurjchem-228	241	10	,	,	PUNCT
eurjchem-228	241	11	h.	h.	PROPN
eurjchem-228	241	12	m.	m.	PROPN
eurjchem-228	241	13	e.	e.	PROPN
eurjchem-228	241	14	;	;	PUNCT
eurjchem-228	241	15	elnagdi	elnagdi	PROPN
eurjchem-228	241	16	,	,	PUNCT
eurjchem-228	241	17	m.	m.	NOUN
eurjchem-228	241	18	h.	h.	PROPN
eurjchem-228	241	19	synthesis	synthesis	PROPN
eurjchem-228	241	20	,	,	PUNCT
eurjchem-228	241	21	2006	2006	NUM
eurjchem-228	241	22	,	,	PUNCT
eurjchem-228	241	23	59‐62	59‐62	NUM
eurjchem-228	241	24	.	.	PUNCT
eurjchem-228	242	1	[	[	X
eurjchem-228	242	2	10	10	NUM
eurjchem-228	242	3	]	]	PUNCT
eurjchem-228	242	4	.	.	PUNCT
eurjchem-228	243	1	murahashi	murahashi	PROPN
eurjchem-228	243	2	,	,	PUNCT
eurjchem-228	243	3	s.	s.	PROPN
eurjchem-228	243	4	;	;	PUNCT
eurjchem-228	243	5	mitsue	mitsue	NOUN
eurjchem-228	243	6	,	,	PUNCT
eurjchem-228	243	7	y.	y.	NOUN
eurjchem-228	243	8	;	;	PUNCT
eurjchem-228	243	9	tsumiyama	tsumiyama	NOUN
eurjchem-228	243	10	,	,	PUNCT
eurjchem-228	243	11	t.	t.	NOUN
eurjchem-228	243	12	bull	bull	NOUN
eurjchem-228	243	13	.	.	PUNCT
eurjchem-228	244	1	chem	chem	NOUN
eurjchem-228	244	2	.	.	PUNCT
eurjchem-228	245	1	soc	soc	PROPN
eurjchem-228	245	2	.	.	PUNCT
eurjchem-228	246	1	jap	jap	PROPN
eurjchem-228	246	2	.	.	PROPN
eurjchem-228	246	3	1987	1987	NUM
eurjchem-228	246	4	,	,	PUNCT
eurjchem-228	246	5	60(9	60(9	NUM
eurjchem-228	246	6	)	)	PUNCT
eurjchem-228	246	7	,	,	PUNCT
eurjchem-228	246	8	3285‐3290	3285‐3290	NUM
eurjchem-228	246	9	.	.	PUNCT
eurjchem-228	247	1	[	[	X
eurjchem-228	247	2	11	11	NUM
eurjchem-228	247	3	]	]	SYM
eurjchem-228	247	4	.	.	PUNCT
eurjchem-228	247	5	braibante	braibante	PROPN
eurjchem-228	247	6	,	,	PUNCT
eurjchem-228	247	7	m.	m.	PROPN
eurjchem-228	247	8	e.	e.	PROPN
eurjchem-228	247	9	f.	f.	PROPN
eurjchem-228	247	10	;	;	PUNCT
eurjchem-228	247	11	braibante	braibante	PROPN
eurjchem-228	247	12	,	,	PUNCT
eurjchem-228	247	13	h.	h.	PROPN
eurjchem-228	247	14	t.	t.	PROPN
eurjchem-228	247	15	s.	s.	PROPN
eurjchem-228	247	16	;	;	PUNCT
eurjchem-228	247	17	rosso	rosso	PROPN
eurjchem-228	247	18	,	,	PUNCT
eurjchem-228	247	19	g.	g.	PROPN
eurjchem-228	247	20	b.	b.	PROPN
eurjchem-228	247	21	;	;	PUNCT
eurjchem-228	247	22	oriques	orique	NOUN
eurjchem-228	247	23	,	,	PUNCT
eurjchem-228	247	24	d.	d.	PROPN
eurjchem-228	247	25	a.	a.	PROPN
eurjchem-228	247	26	j.	j.	PROPN
eurjchem-228	247	27	braz	braz	PROPN
eurjchem-228	247	28	.	.	PUNCT
eurjchem-228	247	29	chem	chem	PROPN
eurjchem-228	247	30	.	.	PUNCT
eurjchem-228	248	1	soc	soc	PROPN
eurjchem-228	248	2	.	.	PUNCT
eurjchem-228	249	1	2003	2003	NUM
eurjchem-228	249	2	,	,	PUNCT
eurjchem-228	249	3	14	14	NUM
eurjchem-228	249	4	,	,	PUNCT
eurjchem-228	249	5	994‐997	994‐997	NUM
eurjchem-228	249	6	.	.	PUNCT
eurjchem-228	250	1	[	[	X
eurjchem-228	250	2	12	12	NUM
eurjchem-228	250	3	]	]	PUNCT
eurjchem-228	250	4	.	.	PUNCT
eurjchem-228	250	5	braibante	braibante	PROPN
eurjchem-228	250	6	,	,	PUNCT
eurjchem-228	250	7	h.	h.	PROPN
eurjchem-228	250	8	t.	t.	PROPN
eurjchem-228	250	9	s.	s.	PROPN
eurjchem-228	250	10	;	;	PUNCT
eurjchem-228	250	11	braibante	braibante	PROPN
eurjchem-228	250	12	,	,	PUNCT
eurjchem-228	250	13	m.	m.	PROPN
eurjchem-228	250	14	e.	e.	PROPN
eurjchem-228	250	15	f.	f.	PROPN
eurjchem-228	250	16	;	;	PUNCT
eurjchem-228	250	17	morel	morel	PROPN
eurjchem-228	250	18	,	,	PUNCT
eurjchem-228	250	19	a.	a.	PROPN
eurjchem-228	250	20	f.	f.	PROPN
eurjchem-228	250	21	;	;	PUNCT
eurjchem-228	250	22	costa	costa	PROPN
eurjchem-228	250	23	.	.	PUNCT
eurjchem-228	251	1	c.	c.	PROPN
eurjchem-228	251	2	c.	c.	PROPN
eurjchem-228	251	3	;	;	PUNCT
eurjchem-228	251	4	lima	lima	PROPN
eurjchem-228	251	5	,	,	PUNCT
eurjchem-228	251	6	m.	m.	NOUN
eurjchem-228	251	7	g.	g.	PROPN
eurjchem-228	251	8	j.	j.	PROPN
eurjchem-228	251	9	braz	braz	PROPN
eurjchem-228	251	10	.	.	PUNCT
eurjchem-228	252	1	chem	chem	PROPN
eurjchem-228	252	2	.	.	PUNCT
eurjchem-228	253	1	soc	soc	PROPN
eurjchem-228	253	2	.	.	PUNCT
eurjchem-228	254	1	2006	2006	NUM
eurjchem-228	254	2	,	,	PUNCT
eurjchem-228	254	3	17	17	NUM
eurjchem-228	254	4	,	,	PUNCT
eurjchem-228	254	5	184‐188	184‐188	NUM
eurjchem-228	254	6	.	.	PUNCT
eurjchem-228	255	1	[	[	X
eurjchem-228	255	2	13	13	NUM
eurjchem-228	255	3	]	]	PUNCT
eurjchem-228	255	4	.	.	PUNCT
eurjchem-228	256	1	rechsteiner	rechsteiner	PROPN
eurjchem-228	256	2	,	,	PUNCT
eurjchem-228	256	3	b.	b.	PROPN
eurjchem-228	256	4	;	;	PUNCT
eurjchem-228	256	5	texier‐boullet	texier‐boullet	PROPN
eurjchem-228	256	6	,	,	PUNCT
eurjchem-228	256	7	f.	f.	PROPN
eurjchem-228	256	8	;	;	PUNCT
eurjchem-228	256	9	hamelin	hamelin	PROPN
eurjchem-228	256	10	,	,	PUNCT
eurjchem-228	256	11	j.	j.	PROPN
eurjchem-228	256	12	tetrahedron	tetrahedron	PROPN
eurjchem-228	256	13	lett	lett	PROPN
eurjchem-228	256	14	.	.	PUNCT
eurjchem-228	257	1	1993	1993	NUM
eurjchem-228	257	2	,	,	PUNCT
eurjchem-228	257	3	34	34	NUM
eurjchem-228	257	4	,	,	PUNCT
eurjchem-228	257	5	5071‐5074	5071‐5074	NUM
eurjchem-228	257	6	.	.	PUNCT
eurjchem-228	258	1	[	[	X
eurjchem-228	258	2	14	14	NUM
eurjchem-228	258	3	]	]	SYM
eurjchem-228	258	4	.	.	PUNCT
eurjchem-228	259	1	lee	lee	PROPN
eurjchem-228	259	2	,	,	PUNCT
eurjchem-228	259	3	d.	d.	PROPN
eurjchem-228	259	4	h.	h.	PROPN
eurjchem-228	259	5	;	;	PUNCT
eurjchem-228	259	6	park	park	PROPN
eurjchem-228	259	7	,	,	PUNCT
eurjchem-228	259	8	s.	s.	PROPN
eurjchem-228	259	9	e.	e.	PROPN
eurjchem-228	259	10	;	;	PUNCT
eurjchem-228	259	11	cho	cho	PROPN
eurjchem-228	259	12	,	,	PUNCT
eurjchem-228	259	13	k.	k.	PROPN
eurjchem-228	259	14	;	;	PUNCT
eurjchem-228	259	15	kim	kim	PROPN
eurjchem-228	259	16	,	,	PUNCT
eurjchem-228	259	17	y.	y.	PROPN
eurjchem-228	259	18	;	;	PUNCT
eurjchem-228	259	19	athar	athar	PROPN
eurjchem-228	259	20	,	,	PUNCT
eurjchem-228	259	21	t.	t.	PROPN
eurjchem-228	259	22	;	;	PUNCT
eurjchem-228	259	23	lee	lee	PROPN
eurjchem-228	259	24	,	,	PUNCT
eurjchem-228	259	25	i.	i.	PROPN
eurjchem-228	259	26	m.	m.	PROPN
eurjchem-228	259	27	tetrahedron	tetrahedron	PROPN
eurjchem-228	259	28	lett	lett	PROPN
eurjchem-228	259	29	.	.	PUNCT
eurjchem-228	260	1	2007	2007	NUM
eurjchem-228	260	2	,	,	PUNCT
eurjchem-228	260	3	48	48	NUM
eurjchem-228	260	4	,	,	PUNCT
eurjchem-228	260	5	8281‐8284	8281‐8284	NUM
eurjchem-228	260	6	.	.	PUNCT
eurjchem-228	261	1	[	[	X
eurjchem-228	261	2	15	15	NUM
eurjchem-228	261	3	]	]	PUNCT
eurjchem-228	261	4	.	.	PUNCT
eurjchem-228	262	1	andrade	andrade	PROPN
eurjchem-228	262	2	,	,	PUNCT
eurjchem-228	262	3	c.	c.	PROPN
eurjchem-228	262	4	k.	k.	PROPN
eurjchem-228	262	5	z.	z.	PROPN
eurjchem-228	262	6	;	;	PUNCT
eurjchem-228	262	7	barreto	barreto	PROPN
eurjchem-228	262	8	,	,	PUNCT
eurjchem-228	262	9	a.	a.	PROPN
eurjchem-228	262	10	s.	s.	PROPN
eurjchem-228	262	11	;	;	PUNCT
eurjchem-228	262	12	silva	silva	PROPN
eurjchem-228	262	13	,	,	PUNCT
eurjchem-228	262	14	w.	w.	PROPN
eurjchem-228	262	15	a.	a.	PROPN
eurjchem-228	262	16	arkivoc	arkivoc	PROPN
eurjchem-228	262	17	2008	2008	NUM
eurjchem-228	262	18	,	,	PUNCT
eurjchem-228	262	19	12	12	NUM
eurjchem-228	262	20	,	,	PUNCT
eurjchem-228	262	21	226‐232	226‐232	NUM
eurjchem-228	262	22	.	.	PUNCT
eurjchem-228	263	1	[	[	X
eurjchem-228	263	2	16	16	NUM
eurjchem-228	263	3	]	]	PUNCT
eurjchem-228	263	4	.	.	PUNCT
eurjchem-228	264	1	al‐mousawi	al‐mousawi	PROPN
eurjchem-228	264	2	,	,	PUNCT
eurjchem-228	264	3	s.	s.	PROPN
eurjchem-228	264	4	m.	m.	PROPN
eurjchem-228	264	5	;	;	PUNCT
eurjchem-228	264	6	el‐apasery	el‐apasery	NOUN
eurjchem-228	264	7	,	,	PUNCT
eurjchem-228	264	8	m.	m.	NOUN
eurjchem-228	264	9	a.	a.	PROPN
eurjchem-228	264	10	;	;	PUNCT
eurjchem-228	264	11	elnagdi	elnagdi	PROPN
eurjchem-228	264	12	,	,	PUNCT
eurjchem-228	264	13	m.	m.	NOUN
eurjchem-228	264	14	h.	h.	PROPN
eurjchem-228	264	15	molecules	molecule	NOUN
eurjchem-228	264	16	2010	2010	NUM
eurjchem-228	264	17	,	,	PUNCT
eurjchem-228	264	18	15	15	NUM
eurjchem-228	264	19	,	,	PUNCT
eurjchem-228	264	20	58‐67	58‐67	NOUN
eurjchem-228	264	21	.	.	PUNCT
eurjchem-228	265	1	[	[	X
eurjchem-228	265	2	17	17	NUM
eurjchem-228	265	3	]	]	PUNCT
eurjchem-228	265	4	.	.	PUNCT
eurjchem-228	265	5	al‐saleh	al‐saleh	NOUN
eurjchem-228	265	6	,	,	PUNCT
eurjchem-228	265	7	b.	b.	PROPN
eurjchem-228	265	8	;	;	PUNCT
eurjchem-228	265	9	el‐apasery	el‐apasery	PROPN
eurjchem-228	265	10	,	,	PUNCT
eurjchem-228	265	11	m.	m.	NOUN
eurjchem-228	265	12	a.	a.	PROPN
eurjchem-228	265	13	;	;	PUNCT
eurjchem-228	265	14	abdel‐aziz	abdel‐aziz	PROPN
eurjchem-228	265	15	,	,	PUNCT
eurjchem-228	265	16	r.	r.	PROPN
eurjchem-228	265	17	s.	s.	PROPN
eurjchem-228	265	18	;	;	PUNCT
eurjchem-228	265	19	elnagdi	elnagdi	PROPN
eurjchem-228	265	20	,	,	PUNCT
eurjchem-228	265	21	m.	m.	PROPN
eurjchem-228	265	22	h.	h.	PROPN
eurjchem-228	265	23	j.	j.	PROPN
eurjchem-228	265	24	heterocycl	heterocycl	PROPN
eurjchem-228	265	25	.	.	PUNCT
eurjchem-228	265	26	chem	chem	PROPN
eurjchem-228	265	27	.	.	PUNCT
eurjchem-228	266	1	2005	2005	NUM
eurjchem-228	266	2	,	,	PUNCT
eurjchem-228	266	3	42(4	42(4	PROPN
eurjchem-228	266	4	)	)	PUNCT
eurjchem-228	266	5	,	,	PUNCT
eurjchem-228	266	6	563‐566	563‐566	NUM
eurjchem-228	266	7	.	.	PUNCT
eurjchem-228	267	1	[	[	X
eurjchem-228	267	2	18	18	NUM
eurjchem-228	267	3	]	]	PUNCT
eurjchem-228	267	4	.	.	PUNCT
eurjchem-228	268	1	el‐dusouqui	el‐dusouqui	NOUN
eurjchem-228	268	2	,	,	PUNCT
eurjchem-228	268	3	o.	o.	PROPN
eurjchem-228	268	4	m.	m.	PROPN
eurjchem-228	268	5	e.	e.	PROPN
eurjchem-228	268	6	;	;	PUNCT
eurjchem-228	268	7	abdelkhalik	abdelkhalik	PROPN
eurjchem-228	268	8	,	,	PUNCT
eurjchem-228	268	9	m.	m.	NOUN
eurjchem-228	268	10	m.	m.	NOUN
eurjchem-228	268	11	;	;	PUNCT
eurjchem-228	268	12	al‐awadi	al‐awadi	NOUN
eurjchem-228	268	13	,	,	PUNCT
eurjchem-228	268	14	n.	n.	PROPN
eurjchem-228	268	15	a.	a.	NOUN
eurjchem-228	268	16	;	;	PUNCT
eurjchem-228	268	17	dib	dib	PROPN
eurjchem-228	268	18	,	,	PUNCT
eurjchem-228	268	19	h.	h.	PROPN
eurjchem-228	268	20	h.	h.	PROPN
eurjchem-228	268	21	;	;	PUNCT
eurjchem-228	268	22	george	george	PROPN
eurjchem-228	268	23	,	,	PUNCT
eurjchem-228	268	24	b.	b.	PROPN
eurjchem-228	268	25	j.	j.	PROPN
eurjchem-228	268	26	;	;	PUNCT
eurjchem-228	268	27	elnagdi	elnagdi	PROPN
eurjchem-228	268	28	,	,	PUNCT
eurjchem-228	268	29	m.	m.	NOUN
eurjchem-228	268	30	h.	h.	PROPN
eurjchem-228	268	31	j.	j.	PROPN
eurjchem-228	268	32	chem	chem	PROPN
eurjchem-228	268	33	.	.	PUNCT
eurjchem-228	269	1	res	re	NOUN
eurjchem-228	269	2	.	.	PUNCT
eurjchem-228	270	1	2006	2006	NUM
eurjchem-228	270	2	,	,	PUNCT
eurjchem-228	270	3	5	5	NUM
eurjchem-228	270	4	,	,	PUNCT
eurjchem-228	270	5	295‐302	295‐302	PROPN
eurjchem-228	270	6	.	.	PUNCT
eurjchem-228	271	1	[	[	X
eurjchem-228	271	2	19	19	NUM
eurjchem-228	271	3	]	]	PUNCT
eurjchem-228	271	4	.	.	PUNCT
eurjchem-228	272	1	martins	martin	NOUN
eurjchem-228	272	2	,	,	PUNCT
eurjchem-228	272	3	m.	m.	NOUN
eurjchem-228	272	4	a.	a.	PROPN
eurjchem-228	272	5	p.	p.	PROPN
eurjchem-228	272	6	;	;	PUNCT
eurjchem-228	272	7	frizzo	frizzo	VERB
eurjchem-228	272	8	,	,	PUNCT
eurjchem-228	272	9	c.	c.	PROPN
eurjchem-228	272	10	p.	p.	PROPN
eurjchem-228	272	11	;	;	PUNCT
eurjchem-228	272	12	moreira	moreira	PROPN
eurjchem-228	272	13	,	,	PUNCT
eurjchem-228	272	14	d.	d.	PROPN
eurjchem-228	272	15	n.	n.	PROPN
eurjchem-228	272	16	;	;	PUNCT
eurjchem-228	273	1	rosa	rosa	PROPN
eurjchem-228	273	2	,	,	PUNCT
eurjchem-228	273	3	f.	f.	PROPN
eurjchem-228	273	4	a.	a.	PROPN
eurjchem-228	273	5	;	;	PUNCT
eurjchem-228	273	6	marzari	marzari	PROPN
eurjchem-228	273	7	,	,	PUNCT
eurjchem-228	273	8	m.	m.	PROPN
eurjchem-228	273	9	r.	r.	PROPN
eurjchem-228	273	10	b.	b.	PROPN
eurjchem-228	273	11	;	;	PUNCT
eurjchem-228	273	12	zanatta	zanatta	PROPN
eurjchem-228	273	13	,	,	PUNCT
eurjchem-228	273	14	n.	n.	PROPN
eurjchem-228	273	15	;	;	PUNCT
eurjchem-228	273	16	bonacorso	bonacorso	PROPN
eurjchem-228	273	17	,	,	PUNCT
eurjchem-228	273	18	h.	h.	PROPN
eurjchem-228	273	19	g.	g.	PROPN
eurjchem-228	273	20	catalysis	catalysis	PROPN
eurjchem-228	273	21	commun	commun	PROPN
eurjchem-228	273	22	.	.	PUNCT
eurjchem-228	273	23	2008	2008	NUM
eurjchem-228	273	24	,	,	PUNCT
eurjchem-228	273	25	9(6	9(6	NUM
eurjchem-228	273	26	)	)	PUNCT
eurjchem-228	273	27	,	,	PUNCT
eurjchem-228	273	28	1375‐	1375‐	NUM
eurjchem-228	273	29	1378	1378	NUM
eurjchem-228	273	30	.	.	PUNCT