id	sid	tid	token	lemma	pos
eurjchem-261	1	1	untitled	untitle	VERB
eurjchem-261	1	2	european	european	PROPN
eurjchem-261	1	3	journal	journal	PROPN
eurjchem-261	1	4	of	of	ADP
eurjchem-261	1	5	chemistry	chemistry	NOUN
eurjchem-261	1	6	2	2	NUM
eurjchem-261	1	7	(	(	PUNCT
eurjchem-261	1	8	2	2	NUM
eurjchem-261	1	9	)	)	PUNCT
eurjchem-261	1	10	(	(	PUNCT
eurjchem-261	1	11	2011	2011	NUM
eurjchem-261	1	12	)	)	PUNCT
eurjchem-261	1	13	269‐271	269‐271	NUM
eurjchem-261	1	14	european	european	ADJ
eurjchem-261	1	15	journal	journal	PROPN
eurjchem-261	1	16	of	of	ADP
eurjchem-261	1	17	chemistry	chemistry	NOUN
eurjchem-261	1	18	issn	issn	PROPN
eurjchem-261	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-261	1	20	(	(	PUNCT
eurjchem-261	1	21	print	print	NOUN
eurjchem-261	1	22	)	)	PUNCT
eurjchem-261	1	23	/	/	SYM
eurjchem-261	1	24	issn	issn	PROPN
eurjchem-261	1	25	2153‐2257	2153‐2257	NUM
eurjchem-261	1	26	(	(	PUNCT
eurjchem-261	1	27	online	online	ADJ
eurjchem-261	1	28	)	)	PUNCT
eurjchem-261	1	29			NOUN
eurjchem-261	1	30	2011	2011	NUM
eurjchem-261	1	31	eurjchem	eurjchem	PROPN
eurjchem-261	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-261	1	33	/	/	SYM
eurjchem-261	1	34	eurjchem.2.2.269‐271.261	eurjchem.2.2.269‐271.261	ADJ
eurjchem-261	1	35	european	european	ADJ
eurjchem-261	1	36	journal	journal	PROPN
eurjchem-261	1	37	of	of	ADP
eurjchem-261	1	38	chemistry	chemistry	PROPN
eurjchem-261	1	39	journal	journal	PROPN
eurjchem-261	1	40	homepage	homepage	NOUN
eurjchem-261	1	41	:	:	PUNCT
eurjchem-261	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-261	1	43	novelties	novelty	NOUN
eurjchem-261	1	44	of	of	ADP
eurjchem-261	1	45	solid‐liquid	solid‐liquid	ADJ
eurjchem-261	1	46	phase	phase	NOUN
eurjchem-261	1	47	transfer	transfer	NOUN
eurjchem-261	1	48	catalyzed	catalyze	VERB
eurjchem-261	1	49	synthesis	synthesis	NOUN
eurjchem-261	1	50	of	of	ADP
eurjchem-261	1	51	benzyl	benzyl	NOUN
eurjchem-261	1	52	diethyl	diethyl	NOUN
eurjchem-261	1	53	phosphate	phosphate	NOUN
eurjchem-261	1	54	from	from	ADP
eurjchem-261	1	55	the	the	DET
eurjchem-261	1	56	sodium	sodium	NOUN
eurjchem-261	1	57	salt	salt	NOUN
eurjchem-261	1	58	of	of	ADP
eurjchem-261	1	59	diethyl	diethyl	NOUN
eurjchem-261	1	60	phosphate	phosphate	NOUN
eurjchem-261	1	61	na	na	PROPN
eurjchem-261	1	62	gea	gea	PROPN
eurjchem-261	1	63	,	,	PUNCT
eurjchem-261	1	64	yumin	yumin	NOUN
eurjchem-261	1	65	zhanga	zhanga	NOUN
eurjchem-261	1	66	,	,	PUNCT
eurjchem-261	1	67	dongmin	dongmin	PROPN
eurjchem-261	1	68	shia	shia	PROPN
eurjchem-261	1	69	,	,	PUNCT
eurjchem-261	1	70	qiang	qiang	PROPN
eurjchem-261	1	71	gua	gua	PROPN
eurjchem-261	1	72	,	,	PUNCT
eurjchem-261	1	73	*	*	PROPN
eurjchem-261	1	74	,	,	PUNCT
eurjchem-261	1	75	xuefeng	xuefeng	PROPN
eurjchem-261	1	76	zhub	zhub	NOUN
eurjchem-261	1	77	and	and	CCONJ
eurjchem-261	1	78	zhiyong	zhiyong	NOUN
eurjchem-261	1	79	dingb	dingb	VERB
eurjchem-261	1	80	a	a	DET
eurjchem-261	1	81	college	college	NOUN
eurjchem-261	1	82	of	of	ADP
eurjchem-261	1	83	chemistry	chemistry	NOUN
eurjchem-261	1	84	,	,	PUNCT
eurjchem-261	1	85	jilin	jilin	PROPN
eurjchem-261	1	86	university	university	PROPN
eurjchem-261	1	87	,	,	PUNCT
eurjchem-261	1	88	changchun	changchun	PROPN
eurjchem-261	1	89	,	,	PUNCT
eurjchem-261	1	90	130012	130012	NUM
eurjchem-261	1	91	,	,	PUNCT
eurjchem-261	1	92	china	china	PROPN
eurjchem-261	1	93	b	b	PROPN
eurjchem-261	1	94	daqing	daqe	VERB
eurjchem-261	1	95	new	new	ADJ
eurjchem-261	1	96	century	century	NOUN
eurjchem-261	1	97	fine	fine	PROPN
eurjchem-261	1	98	chemicals	chemicals	PROPN
eurjchem-261	1	99	co.	co.	PROPN
eurjchem-261	1	100	ltd	ltd	PROPN
eurjchem-261	1	101	.	.	PROPN
eurjchem-261	1	102	,	,	PUNCT
eurjchem-261	1	103	daqing	daqing	NOUN
eurjchem-261	1	104	,	,	PUNCT
eurjchem-261	1	105	heilongjiang	heilongjiang	PROPN
eurjchem-261	1	106	province	province	NOUN
eurjchem-261	1	107	,	,	PUNCT
eurjchem-261	1	108	163511	163511	NUM
eurjchem-261	1	109	,	,	PUNCT
eurjchem-261	1	110	china	china	PROPN
eurjchem-261	1	111	*	*	PUNCT
eurjchem-261	1	112	corresponding	correspond	VERB
eurjchem-261	1	113	author	author	NOUN
eurjchem-261	1	114	at	at	ADP
eurjchem-261	1	115	:	:	PUNCT
eurjchem-261	1	116	college	college	NOUN
eurjchem-261	1	117	of	of	ADP
eurjchem-261	1	118	chemistry	chemistry	PROPN
eurjchem-261	1	119	,	,	PUNCT
eurjchem-261	1	120	jilin	jilin	PROPN
eurjchem-261	1	121	university	university	PROPN
eurjchem-261	1	122	,	,	PUNCT
eurjchem-261	1	123	changchun	changchun	PROPN
eurjchem-261	1	124	,	,	PUNCT
eurjchem-261	1	125	130012	130012	NUM
eurjchem-261	1	126	,	,	PUNCT
eurjchem-261	1	127	china	china	PROPN
eurjchem-261	1	128	.	.	PUNCT
eurjchem-261	2	1	tel	tel	PROPN
eurjchem-261	2	2	.	.	PUNCT
eurjchem-261	2	3	:	:	PUNCT
eurjchem-261	3	1	+86.431.85168470(3	+86.431.85168470(3	NOUN
eurjchem-261	3	2	)	)	PUNCT
eurjchem-261	3	3	;	;	PUNCT
eurjchem-261	3	4	fax	fax	NOUN
eurjchem-261	3	5	:	:	PUNCT
eurjchem-261	3	6	+86.431.85168420	+86.431.85168420	NUM
eurjchem-261	3	7	.	.	PUNCT
eurjchem-261	3	8	e‐mail	e‐mail	PUNCT
eurjchem-261	4	1	address	address	NOUN
eurjchem-261	4	2	:	:	PUNCT
eurjchem-261	4	3	guqiang@jlu.edu.cn	guqiang@jlu.edu.cn	PROPN
eurjchem-261	4	4	(	(	PUNCT
eurjchem-261	4	5	q.	q.	PROPN
eurjchem-261	4	6	gu	gu	PROPN
eurjchem-261	4	7	)	)	PUNCT
eurjchem-261	4	8	.	.	PUNCT
eurjchem-261	5	1	communication	communication	NOUN
eurjchem-261	5	2	information	information	NOUN
eurjchem-261	5	3	abstract	abstract	ADJ
eurjchem-261	5	4	received	receive	VERB
eurjchem-261	5	5	:	:	PUNCT
eurjchem-261	5	6	24	24	NUM
eurjchem-261	5	7	august	august	PROPN
eurjchem-261	5	8	2010	2010	NUM
eurjchem-261	5	9	received	receive	VERB
eurjchem-261	5	10	in	in	ADP
eurjchem-261	5	11	revised	revise	VERB
eurjchem-261	5	12	form	form	NOUN
eurjchem-261	5	13	:	:	PUNCT
eurjchem-261	5	14	29	29	NUM
eurjchem-261	5	15	november	november	NOUN
eurjchem-261	5	16	2010	2010	NUM
eurjchem-261	5	17	accepted	accept	VERB
eurjchem-261	5	18	:	:	PUNCT
eurjchem-261	6	1	08	08	NUM
eurjchem-261	6	2	december	december	PROPN
eurjchem-261	6	3	2010	2010	NUM
eurjchem-261	6	4	online	online	NOUN
eurjchem-261	6	5	:	:	PUNCT
eurjchem-261	6	6	30	30	NUM
eurjchem-261	6	7	june	june	PROPN
eurjchem-261	6	8	2011	2011	NUM
eurjchem-261	6	9	keywords	keyword	NOUN
eurjchem-261	6	10	solid‐liquid	solid‐liquid	ADJ
eurjchem-261	6	11	phase	phase	NOUN
eurjchem-261	6	12	transfer	transfer	NOUN
eurjchem-261	6	13	catalysis	catalysis	NOUN
eurjchem-261	6	14	coupled	couple	VERB
eurjchem-261	6	15	with	with	ADP
eurjchem-261	6	16	mixed	mixed	ADJ
eurjchem-261	6	17	solvents	solvent	NOUN
eurjchem-261	6	18	,	,	PUNCT
eurjchem-261	6	19	which	which	PRON
eurjchem-261	6	20	could	could	AUX
eurjchem-261	6	21	be	be	AUX
eurjchem-261	6	22	recycled	recycle	VERB
eurjchem-261	6	23	,	,	PUNCT
eurjchem-261	6	24	as	as	ADP
eurjchem-261	6	25	a	a	DET
eurjchem-261	6	26	green	green	ADJ
eurjchem-261	6	27	chemistry	chemistry	NOUN
eurjchem-261	6	28	procedure	procedure	NOUN
eurjchem-261	6	29	,	,	PUNCT
eurjchem-261	6	30	was	be	AUX
eurjchem-261	6	31	applied	apply	VERB
eurjchem-261	6	32	to	to	ADP
eurjchem-261	6	33	the	the	DET
eurjchem-261	6	34	synthesis	synthesis	NOUN
eurjchem-261	6	35	of	of	ADP
eurjchem-261	6	36	phosphate	phosphate	NOUN
eurjchem-261	6	37	from	from	ADP
eurjchem-261	6	38	the	the	DET
eurjchem-261	6	39	sodium	sodium	NOUN
eurjchem-261	6	40	salt	salt	NOUN
eurjchem-261	6	41	of	of	ADP
eurjchem-261	6	42	diethyl	diethyl	NOUN
eurjchem-261	6	43	phosphate	phosphate	NOUN
eurjchem-261	6	44	.	.	PUNCT
eurjchem-261	7	1	the	the	DET
eurjchem-261	7	2	benzyl	benzyl	NOUN
eurjchem-261	7	3	diethyl	diethyl	NOUN
eurjchem-261	7	4	phosphate	phosphate	NOUN
eurjchem-261	7	5	was	be	AUX
eurjchem-261	7	6	synthesized	synthesize	VERB
eurjchem-261	7	7	in	in	ADP
eurjchem-261	7	8	good	good	ADJ
eurjchem-261	7	9	yield	yield	NOUN
eurjchem-261	7	10	via	via	ADP
eurjchem-261	7	11	one‐pot	one‐pot	NOUN
eurjchem-261	7	12	method	method	NOUN
eurjchem-261	7	13	from	from	ADP
eurjchem-261	7	14	the	the	DET
eurjchem-261	7	15	reaction	reaction	NOUN
eurjchem-261	7	16	of	of	ADP
eurjchem-261	7	17	the	the	DET
eurjchem-261	7	18	industrial	industrial	ADJ
eurjchem-261	7	19	by‐product	by‐product	PROPN
eurjchem-261	7	20	sodium	sodium	NOUN
eurjchem-261	7	21	salt	salt	NOUN
eurjchem-261	7	22	of	of	ADP
eurjchem-261	7	23	diethyl	diethyl	NOUN
eurjchem-261	7	24	phosphate	phosphate	NOUN
eurjchem-261	7	25	with	with	ADP
eurjchem-261	7	26	benzyl	benzyl	NOUN
eurjchem-261	7	27	chloride	chloride	NOUN
eurjchem-261	7	28	in	in	ADP
eurjchem-261	7	29	solid‐liquid	solid‐liquid	ADJ
eurjchem-261	7	30	phase	phase	NOUN
eurjchem-261	7	31	transfer	transfer	NOUN
eurjchem-261	7	32	catalysis	catalysis	NOUN
eurjchem-261	7	33	and	and	CCONJ
eurjchem-261	7	34	toluene‐water	toluene‐water	NOUN
eurjchem-261	7	35	mixed	mixed	ADJ
eurjchem-261	7	36	solvents	solvent	NOUN
eurjchem-261	7	37	.	.	PUNCT
eurjchem-261	8	1	the	the	DET
eurjchem-261	8	2	effects	effect	NOUN
eurjchem-261	8	3	of	of	ADP
eurjchem-261	8	4	catalyst	catalyst	NOUN
eurjchem-261	8	5	structure	structure	NOUN
eurjchem-261	8	6	,	,	PUNCT
eurjchem-261	8	7	the	the	DET
eurjchem-261	8	8	amounts	amount	NOUN
eurjchem-261	8	9	of	of	ADP
eurjchem-261	8	10	catalyst	catalyst	NOUN
eurjchem-261	8	11	,	,	PUNCT
eurjchem-261	8	12	the	the	DET
eurjchem-261	8	13	raw	raw	ADJ
eurjchem-261	8	14	material	material	NOUN
eurjchem-261	8	15	molar	molar	ADJ
eurjchem-261	8	16	ratio	ratio	NOUN
eurjchem-261	8	17	,	,	PUNCT
eurjchem-261	8	18	water	water	NOUN
eurjchem-261	8	19	loading	loading	NOUN
eurjchem-261	8	20	,	,	PUNCT
eurjchem-261	8	21	and	and	CCONJ
eurjchem-261	8	22	reaction	reaction	NOUN
eurjchem-261	8	23	temperature	temperature	NOUN
eurjchem-261	8	24	on	on	ADP
eurjchem-261	8	25	the	the	DET
eurjchem-261	8	26	conversion	conversion	NOUN
eurjchem-261	8	27	of	of	ADP
eurjchem-261	8	28	the	the	DET
eurjchem-261	8	29	reaction	reaction	NOUN
eurjchem-261	8	30	were	be	AUX
eurjchem-261	8	31	investigated	investigate	VERB
eurjchem-261	8	32	.	.	PUNCT
eurjchem-261	9	1	the	the	DET
eurjchem-261	9	2	structure	structure	NOUN
eurjchem-261	9	3	of	of	ADP
eurjchem-261	9	4	the	the	DET
eurjchem-261	9	5	benzyl	benzyl	NOUN
eurjchem-261	9	6	diethyl	diethyl	NOUN
eurjchem-261	9	7	phosphate	phosphate	NOUN
eurjchem-261	9	8	generated	generate	VERB
eurjchem-261	9	9	was	be	AUX
eurjchem-261	9	10	confirmed	confirm	VERB
eurjchem-261	9	11	by	by	ADP
eurjchem-261	9	12	elemental	elemental	ADJ
eurjchem-261	9	13	analysis	analysis	NOUN
eurjchem-261	9	14	,	,	PUNCT
eurjchem-261	9	15	ir	ir	INTJ
eurjchem-261	9	16	,	,	PUNCT
eurjchem-261	9	17	1h	1h	NUM
eurjchem-261	9	18	nmr	nmr	NOUN
eurjchem-261	9	19	and	and	CCONJ
eurjchem-261	9	20	gc	gc	PROPN
eurjchem-261	9	21	/	/	SYM
eurjchem-261	9	22	ms	ms	PROPN
eurjchem-261	9	23	.	.	PROPN
eurjchem-261	9	24	benzyl	benzyl	PROPN
eurjchem-261	9	25	diethyl	diethyl	NOUN
eurjchem-261	9	26	phosphate	phosphate	NOUN
eurjchem-261	9	27	sodium	sodium	NOUN
eurjchem-261	9	28	salt	salt	NOUN
eurjchem-261	9	29	of	of	ADP
eurjchem-261	9	30	diethyl	diethyl	NOUN
eurjchem-261	9	31	phosphate	phosphate	ADJ
eurjchem-261	9	32	solid‐liquid	solid‐liquid	ADJ
eurjchem-261	9	33	phase	phase	NOUN
eurjchem-261	9	34	transfer	transfer	NOUN
eurjchem-261	9	35	catalysis	catalysis	NOUN
eurjchem-261	9	36	nucleophilic	nucleophilic	ADJ
eurjchem-261	9	37	substitution	substitution	NOUN
eurjchem-261	9	38	organic	organic	ADJ
eurjchem-261	9	39	phosphate	phosphate	NOUN
eurjchem-261	9	40	mechanism	mechanism	NOUN
eurjchem-261	9	41	1	1	NUM
eurjchem-261	9	42	.	.	PUNCT
eurjchem-261	10	1	introduction	introduction	NOUN
eurjchem-261	10	2	organic	organic	ADJ
eurjchem-261	10	3	phosphates	phosphate	NOUN
eurjchem-261	10	4	play	play	VERB
eurjchem-261	10	5	an	an	DET
eurjchem-261	10	6	important	important	ADJ
eurjchem-261	10	7	role	role	NOUN
eurjchem-261	10	8	in	in	ADP
eurjchem-261	10	9	a	a	DET
eurjchem-261	10	10	variety	variety	NOUN
eurjchem-261	10	11	of	of	ADP
eurjchem-261	10	12	chemical	chemical	NOUN
eurjchem-261	10	13	processes	process	NOUN
eurjchem-261	10	14	,	,	PUNCT
eurjchem-261	10	15	such	such	ADJ
eurjchem-261	10	16	as	as	ADP
eurjchem-261	10	17	catalysts	catalyst	NOUN
eurjchem-261	10	18	for	for	ADP
eurjchem-261	10	19	condensation	condensation	NOUN
eurjchem-261	10	20	reaction	reaction	NOUN
eurjchem-261	10	21	[	[	X
eurjchem-261	10	22	1	1	X
eurjchem-261	10	23	]	]	PUNCT
eurjchem-261	10	24	and	and	CCONJ
eurjchem-261	10	25	epoxidation	epoxidation	NOUN
eurjchem-261	10	26	reaction	reaction	NOUN
eurjchem-261	10	27	[	[	X
eurjchem-261	10	28	2	2	NUM
eurjchem-261	10	29	]	]	PUNCT
eurjchem-261	10	30	,	,	PUNCT
eurjchem-261	10	31	pro‐drugs	pro‐drug	NOUN
eurjchem-261	10	32	[	[	X
eurjchem-261	10	33	3	3	X
eurjchem-261	10	34	]	]	PUNCT
eurjchem-261	10	35	to	to	PART
eurjchem-261	10	36	increase	increase	VERB
eurjchem-261	10	37	the	the	DET
eurjchem-261	10	38	water	water	NOUN
eurjchem-261	10	39	solubility	solubility	NOUN
eurjchem-261	10	40	and	and	CCONJ
eurjchem-261	10	41	bio‐availability	bio‐availability	NOUN
eurjchem-261	10	42	of	of	ADP
eurjchem-261	10	43	the	the	DET
eurjchem-261	10	44	agents	agent	NOUN
eurjchem-261	10	45	in	in	ADP
eurjchem-261	10	46	biological	biological	ADJ
eurjchem-261	10	47	chemistry	chemistry	NOUN
eurjchem-261	11	1	[	[	X
eurjchem-261	11	2	4	4	NUM
eurjchem-261	11	3	]	]	PUNCT
eurjchem-261	11	4	,	,	PUNCT
eurjchem-261	11	5	solvent	solvent	ADJ
eurjchem-261	11	6	extraction	extraction	NOUN
eurjchem-261	11	7	processes	process	NOUN
eurjchem-261	11	8	and	and	CCONJ
eurjchem-261	11	9	insecticides	insecticide	NOUN
eurjchem-261	11	10	in	in	ADP
eurjchem-261	11	11	agriculture	agriculture	NOUN
eurjchem-261	11	12	applications	application	NOUN
eurjchem-261	12	1	[	[	X
eurjchem-261	12	2	5	5	NUM
eurjchem-261	12	3	]	]	PUNCT
eurjchem-261	12	4	,	,	PUNCT
eurjchem-261	12	5	and	and	CCONJ
eurjchem-261	12	6	so	so	ADV
eurjchem-261	12	7	on	on	ADV
eurjchem-261	12	8	.	.	PUNCT
eurjchem-261	13	1	the	the	DET
eurjchem-261	13	2	preparation	preparation	NOUN
eurjchem-261	13	3	of	of	ADP
eurjchem-261	13	4	most	most	ADJ
eurjchem-261	13	5	phosphates	phosphate	NOUN
eurjchem-261	13	6	is	be	AUX
eurjchem-261	13	7	based	base	VERB
eurjchem-261	13	8	on	on	ADP
eurjchem-261	13	9	the	the	DET
eurjchem-261	13	10	phosphorylation	phosphorylation	NOUN
eurjchem-261	13	11	of	of	ADP
eurjchem-261	13	12	alcohols	alcohol	NOUN
eurjchem-261	13	13	or	or	CCONJ
eurjchem-261	13	14	phenols	phenol	NOUN
eurjchem-261	13	15	with	with	ADP
eurjchem-261	13	16	some	some	DET
eurjchem-261	13	17	sort	sort	NOUN
eurjchem-261	13	18	of	of	ADP
eurjchem-261	13	19	“	"	PUNCT
eurjchem-261	13	20	activated	activate	VERB
eurjchem-261	13	21	phosphoric	phosphoric	NOUN
eurjchem-261	13	22	acid	acid	NOUN
eurjchem-261	13	23	”	"	PUNCT
eurjchem-261	13	24	in	in	ADP
eurjchem-261	13	25	the	the	DET
eurjchem-261	13	26	literature	literature	NOUN
eurjchem-261	13	27	[	[	X
eurjchem-261	13	28	6‐9	6‐9	NOUN
eurjchem-261	13	29	]	]	PUNCT
eurjchem-261	13	30	.	.	PUNCT
eurjchem-261	14	1	recently	recently	ADV
eurjchem-261	14	2	,	,	PUNCT
eurjchem-261	14	3	the	the	DET
eurjchem-261	14	4	cross‐coupling	cross‐couple	VERB
eurjchem-261	14	5	reaction	reaction	NOUN
eurjchem-261	14	6	of	of	ADP
eurjchem-261	14	7	substituted	substitute	VERB
eurjchem-261	14	8	benzyl	benzyl	NOUN
eurjchem-261	14	9	diethyl	diethyl	NOUN
eurjchem-261	14	10	phosphates	phosphate	NOUN
eurjchem-261	14	11	with	with	ADP
eurjchem-261	14	12	arylboronic	arylboronic	ADJ
eurjchem-261	14	13	acids	acid	NOUN
eurjchem-261	14	14	and	and	CCONJ
eurjchem-261	14	15	arylmagnesium	arylmagnesium	NOUN
eurjchem-261	14	16	reagents	reagent	NOUN
eurjchem-261	14	17	has	have	AUX
eurjchem-261	14	18	been	be	AUX
eurjchem-261	14	19	explored	explore	VERB
eurjchem-261	14	20	by	by	ADP
eurjchem-261	14	21	mclaughlin	mclaughlin	PROPN
eurjchem-261	14	22	[	[	X
eurjchem-261	14	23	10	10	NUM
eurjchem-261	14	24	]	]	PUNCT
eurjchem-261	14	25	and	and	CCONJ
eurjchem-261	14	26	kofink	kofink	VERB
eurjchem-261	14	27	et	et	PROPN
eurjchem-261	14	28	al	al	PROPN
eurjchem-261	14	29	.	.	PUNCT
eurjchem-261	15	1	[	[	X
eurjchem-261	15	2	11	11	NUM
eurjchem-261	15	3	]	]	PUNCT
eurjchem-261	15	4	,	,	PUNCT
eurjchem-261	15	5	respectively	respectively	ADV
eurjchem-261	15	6	.	.	PUNCT
eurjchem-261	16	1	the	the	DET
eurjchem-261	16	2	generally	generally	ADV
eurjchem-261	16	3	reported	report	VERB
eurjchem-261	16	4	method	method	NOUN
eurjchem-261	16	5	for	for	ADP
eurjchem-261	16	6	the	the	DET
eurjchem-261	16	7	preparation	preparation	NOUN
eurjchem-261	16	8	of	of	ADP
eurjchem-261	16	9	a	a	DET
eurjchem-261	16	10	series	series	NOUN
eurjchem-261	16	11	of	of	ADP
eurjchem-261	16	12	substituted	substitute	VERB
eurjchem-261	16	13	benzyl	benzyl	NOUN
eurjchem-261	16	14	diethyl	diethyl	NOUN
eurjchem-261	16	15	phosphates	phosphate	NOUN
eurjchem-261	16	16	was	be	AUX
eurjchem-261	16	17	the	the	DET
eurjchem-261	16	18	corresponding	corresponding	ADJ
eurjchem-261	16	19	substituted	substitute	VERB
eurjchem-261	16	20	benzyl	benzyl	NOUN
eurjchem-261	16	21	alcohols	alcohol	NOUN
eurjchem-261	16	22	by	by	ADP
eurjchem-261	16	23	phosphorylation	phosphorylation	NOUN
eurjchem-261	16	24	with	with	ADP
eurjchem-261	16	25	diethyl	diethyl	NOUN
eurjchem-261	16	26	chloro‐phosphate	chloro‐phosphate	NOUN
eurjchem-261	16	27	in	in	ADP
eurjchem-261	16	28	the	the	DET
eurjchem-261	16	29	presence	presence	NOUN
eurjchem-261	16	30	of	of	ADP
eurjchem-261	16	31	triethylamine	triethylamine	NOUN
eurjchem-261	16	32	or	or	CCONJ
eurjchem-261	16	33	pyridine	pyridine	NOUN
eurjchem-261	16	34	,	,	PUNCT
eurjchem-261	16	35	and	and	CCONJ
eurjchem-261	16	36	the	the	DET
eurjchem-261	16	37	yields	yield	NOUN
eurjchem-261	16	38	were	be	AUX
eurjchem-261	16	39	low	low	ADJ
eurjchem-261	16	40	[	[	X
eurjchem-261	16	41	12‐14	12‐14	X
eurjchem-261	16	42	]	]	PUNCT
eurjchem-261	16	43	.	.	PUNCT
eurjchem-261	17	1	clearly	clearly	ADV
eurjchem-261	17	2	,	,	PUNCT
eurjchem-261	17	3	there	there	PRON
eurjchem-261	17	4	is	be	VERB
eurjchem-261	17	5	a	a	DET
eurjchem-261	17	6	need	need	NOUN
eurjchem-261	17	7	for	for	ADP
eurjchem-261	17	8	improving	improve	VERB
eurjchem-261	17	9	synthesis	synthesis	NOUN
eurjchem-261	17	10	of	of	ADP
eurjchem-261	17	11	substituted	substitute	VERB
eurjchem-261	17	12	benzyl	benzyl	NOUN
eurjchem-261	17	13	diethyl	diethyl	NOUN
eurjchem-261	17	14	phosphates	phosphate	NOUN
eurjchem-261	17	15	.	.	PUNCT
eurjchem-261	18	1	it	it	PRON
eurjchem-261	18	2	is	be	AUX
eurjchem-261	18	3	known	know	VERB
eurjchem-261	18	4	that	that	SCONJ
eurjchem-261	18	5	sodium	sodium	NOUN
eurjchem-261	18	6	salt	salt	NOUN
eurjchem-261	18	7	of	of	ADP
eurjchem-261	18	8	diethyl	diethyl	NOUN
eurjchem-261	18	9	phosphate	phosphate	NOUN
eurjchem-261	18	10	was	be	AUX
eurjchem-261	18	11	very	very	ADV
eurjchem-261	18	12	poor	poor	ADJ
eurjchem-261	18	13	nucleophilic	nucleophilic	ADJ
eurjchem-261	18	14	agent	agent	NOUN
eurjchem-261	18	15	and	and	CCONJ
eurjchem-261	18	16	its	its	PRON
eurjchem-261	18	17	nucleophilic	nucleophilic	ADJ
eurjchem-261	18	18	substitution	substitution	NOUN
eurjchem-261	18	19	with	with	ADP
eurjchem-261	18	20	organic	organic	ADJ
eurjchem-261	18	21	halides	halide	NOUN
eurjchem-261	18	22	was	be	AUX
eurjchem-261	18	23	rarely	rarely	ADV
eurjchem-261	18	24	studied	study	VERB
eurjchem-261	18	25	to	to	PART
eurjchem-261	18	26	be	be	AUX
eurjchem-261	18	27	of	of	ADP
eurjchem-261	18	28	any	any	DET
eurjchem-261	18	29	preparative	preparative	ADJ
eurjchem-261	18	30	importance	importance	NOUN
eurjchem-261	19	1	[	[	X
eurjchem-261	19	2	15	15	NUM
eurjchem-261	19	3	]	]	PUNCT
eurjchem-261	19	4	.	.	PUNCT
eurjchem-261	20	1	the	the	DET
eurjchem-261	20	2	sodium	sodium	NOUN
eurjchem-261	20	3	salt	salt	NOUN
eurjchem-261	20	4	of	of	ADP
eurjchem-261	20	5	diethyl	diethyl	NOUN
eurjchem-261	20	6	phosphate	phosphate	NOUN
eurjchem-261	20	7	is	be	AUX
eurjchem-261	20	8	an	an	DET
eurjchem-261	20	9	inconveniently	inconveniently	ADV
eurjchem-261	20	10	disposed	dispose	VERB
eurjchem-261	20	11	and	and	CCONJ
eurjchem-261	20	12	contaminates	contaminate	VERB
eurjchem-261	20	13	environment	environment	NOUN
eurjchem-261	20	14	side‐product	side‐product	NOUN
eurjchem-261	20	15	of	of	ADP
eurjchem-261	20	16	industrial	industrial	ADJ
eurjchem-261	20	17	products	product	NOUN
eurjchem-261	20	18	,	,	PUNCT
eurjchem-261	20	19	which	which	PRON
eurjchem-261	20	20	derive	derive	VERB
eurjchem-261	20	21	from	from	ADP
eurjchem-261	20	22	fluorescent	fluorescent	ADJ
eurjchem-261	20	23	brightener	brightener	NOUN
eurjchem-261	20	24	2,2'‐(2,2'‐(1,4‐phenylene	2,2'‐(2,2'‐(1,4‐phenylene	NUM
eurjchem-261	20	25	)	)	PUNCT
eurjchem-261	20	26	bis(ethene‐2,1‐diyl	bis(ethene‐2,1‐diyl	NOUN
eurjchem-261	20	27	)	)	PUNCT
eurjchem-261	20	28	)	)	PUNCT
eurjchem-261	20	29	dibenzonitrile	dibenzonitrile	NOUN
eurjchem-261	20	30	(	(	PUNCT
eurjchem-261	20	31	er	er	INTJ
eurjchem-261	20	32	)	)	PUNCT
eurjchem-261	20	33	by	by	ADP
eurjchem-261	20	34	employing	employ	VERB
eurjchem-261	20	35	triethyl	triethyl	PROPN
eurjchem-261	20	36	phosphite	phosphite	PROPN
eurjchem-261	20	37	as	as	ADP
eurjchem-261	20	38	catalyst	catalyst	NOUN
eurjchem-261	20	39	,	,	PUNCT
eurjchem-261	20	40	and	and	CCONJ
eurjchem-261	20	41	increases	increase	VERB
eurjchem-261	20	42	year	year	NOUN
eurjchem-261	20	43	after	after	ADP
eurjchem-261	20	44	year	year	NOUN
eurjchem-261	20	45	.	.	PUNCT
eurjchem-261	21	1	therefore	therefore	ADV
eurjchem-261	21	2	,	,	PUNCT
eurjchem-261	21	3	it	it	PRON
eurjchem-261	21	4	is	be	AUX
eurjchem-261	21	5	more	more	ADV
eurjchem-261	21	6	important	important	ADJ
eurjchem-261	21	7	to	to	PART
eurjchem-261	21	8	utilize	utilize	VERB
eurjchem-261	21	9	sodium	sodium	NOUN
eurjchem-261	21	10	salt	salt	NOUN
eurjchem-261	21	11	of	of	ADP
eurjchem-261	21	12	diethyl	diethyl	NOUN
eurjchem-261	21	13	phosphate	phosphate	NOUN
eurjchem-261	21	14	,	,	PUNCT
eurjchem-261	21	15	which	which	PRON
eurjchem-261	21	16	not	not	PART
eurjchem-261	21	17	only	only	ADV
eurjchem-261	21	18	reduce	reduce	VERB
eurjchem-261	21	19	environmental	environmental	ADJ
eurjchem-261	21	20	pollution	pollution	NOUN
eurjchem-261	21	21	but	but	CCONJ
eurjchem-261	21	22	also	also	ADV
eurjchem-261	21	23	bring	bring	VERB
eurjchem-261	21	24	out	out	ADP
eurjchem-261	21	25	considerable	considerable	ADJ
eurjchem-261	21	26	economic	economic	ADJ
eurjchem-261	21	27	value	value	NOUN
eurjchem-261	21	28	.	.	PUNCT
eurjchem-261	22	1	to	to	ADP
eurjchem-261	22	2	the	the	DET
eurjchem-261	22	3	best	good	ADJ
eurjchem-261	22	4	of	of	ADP
eurjchem-261	22	5	our	our	PRON
eurjchem-261	22	6	knowledge	knowledge	NOUN
eurjchem-261	22	7	,	,	PUNCT
eurjchem-261	22	8	the	the	DET
eurjchem-261	22	9	research	research	NOUN
eurjchem-261	22	10	on	on	ADP
eurjchem-261	22	11	sodium	sodium	NOUN
eurjchem-261	22	12	salt	salt	NOUN
eurjchem-261	22	13	of	of	ADP
eurjchem-261	22	14	diethyl	diethyl	NOUN
eurjchem-261	22	15	phosphate	phosphate	NOUN
eurjchem-261	22	16	reused	reuse	VERB
eurjchem-261	22	17	and	and	CCONJ
eurjchem-261	22	18	prepared	prepare	VERB
eurjchem-261	22	19	available	available	ADJ
eurjchem-261	22	20	organic	organic	ADJ
eurjchem-261	22	21	phosphate	phosphate	NOUN
eurjchem-261	22	22	has	have	AUX
eurjchem-261	22	23	hardly	hardly	ADV
eurjchem-261	22	24	been	be	AUX
eurjchem-261	22	25	reported	report	VERB
eurjchem-261	22	26	.	.	PUNCT
eurjchem-261	23	1	it	it	PRON
eurjchem-261	23	2	is	be	AUX
eurjchem-261	23	3	now	now	ADV
eurjchem-261	23	4	demonstrated	demonstrate	VERB
eurjchem-261	23	5	that	that	DET
eurjchem-261	23	6	phosphorylation	phosphorylation	NOUN
eurjchem-261	23	7	of	of	ADP
eurjchem-261	23	8	benzyl	benzyl	NOUN
eurjchem-261	23	9	chloride	chloride	NOUN
eurjchem-261	23	10	(	(	PUNCT
eurjchem-261	23	11	2	2	NUM
eurjchem-261	23	12	)	)	PUNCT
eurjchem-261	23	13	by	by	ADP
eurjchem-261	23	14	means	mean	NOUN
eurjchem-261	23	15	of	of	ADP
eurjchem-261	23	16	sodium	sodium	NOUN
eurjchem-261	23	17	salt	salt	NOUN
eurjchem-261	23	18	of	of	ADP
eurjchem-261	23	19	diethyl	diethyl	NOUN
eurjchem-261	23	20	phosphate	phosphate	NOUN
eurjchem-261	23	21	(	(	PUNCT
eurjchem-261	23	22	1	1	NUM
eurjchem-261	23	23	)	)	PUNCT
eurjchem-261	23	24	in	in	ADP
eurjchem-261	23	25	toluene‐water	toluene‐water	NOUN
eurjchem-261	23	26	at	at	ADP
eurjchem-261	23	27	reflux	reflux	NOUN
eurjchem-261	23	28	temperature	temperature	NOUN
eurjchem-261	23	29	in	in	ADP
eurjchem-261	23	30	solid‐liquid	solid‐liquid	ADJ
eurjchem-261	23	31	system	system	NOUN
eurjchem-261	23	32	with	with	ADP
eurjchem-261	23	33	tetrabutyl	tetrabutyl	NOUN
eurjchem-261	23	34	ammonium	ammonium	NOUN
eurjchem-261	23	35	bromide	bromide	NOUN
eurjchem-261	23	36	(	(	PUNCT
eurjchem-261	23	37	tbab	tbab	PROPN
eurjchem-261	23	38	)	)	PUNCT
eurjchem-261	23	39	,	,	PUNCT
eurjchem-261	23	40	affording	afford	VERB
eurjchem-261	23	41	the	the	DET
eurjchem-261	23	42	good	good	ADJ
eurjchem-261	23	43	yield	yield	NOUN
eurjchem-261	23	44	of	of	ADP
eurjchem-261	23	45	benzyl	benzyl	NOUN
eurjchem-261	23	46	diethyl	diethyl	NOUN
eurjchem-261	23	47	phosphate	phosphate	NOUN
eurjchem-261	23	48	(	(	PUNCT
eurjchem-261	23	49	3	3	NUM
eurjchem-261	23	50	)	)	PUNCT
eurjchem-261	23	51	(	(	PUNCT
eurjchem-261	23	52	scheme	scheme	NOUN
eurjchem-261	23	53	1	1	NUM
eurjchem-261	23	54	)	)	PUNCT
eurjchem-261	23	55	.	.	PUNCT
eurjchem-261	24	1	this	this	DET
eurjchem-261	24	2	one‐pot	one‐pot	NOUN
eurjchem-261	24	3	procedure	procedure	NOUN
eurjchem-261	24	4	is	be	AUX
eurjchem-261	24	5	a	a	DET
eurjchem-261	24	6	facile	facile	ADJ
eurjchem-261	24	7	and	and	CCONJ
eurjchem-261	24	8	efficient	efficient	ADJ
eurjchem-261	24	9	method	method	NOUN
eurjchem-261	24	10	for	for	ADP
eurjchem-261	24	11	the	the	DET
eurjchem-261	24	12	synthesis	synthesis	NOUN
eurjchem-261	24	13	of	of	ADP
eurjchem-261	24	14	benzyl	benzyl	NOUN
eurjchem-261	24	15	diethyl	diethyl	NOUN
eurjchem-261	24	16	phosphate	phosphate	NOUN
eurjchem-261	24	17	,	,	PUNCT
eurjchem-261	24	18	with	with	ADP
eurjchem-261	24	19	the	the	DET
eurjchem-261	24	20	advantages	advantage	NOUN
eurjchem-261	24	21	of	of	ADP
eurjchem-261	24	22	mild	mild	ADJ
eurjchem-261	24	23	reaction	reaction	NOUN
eurjchem-261	24	24	conditions	condition	NOUN
eurjchem-261	24	25	,	,	PUNCT
eurjchem-261	24	26	simple	simple	ADJ
eurjchem-261	24	27	operations	operation	NOUN
eurjchem-261	24	28	,	,	PUNCT
eurjchem-261	24	29	clean	clean	ADJ
eurjchem-261	24	30	technology	technology	NOUN
eurjchem-261	24	31	and	and	CCONJ
eurjchem-261	24	32	high	high	ADJ
eurjchem-261	24	33	yields	yield	NOUN
eurjchem-261	24	34	.	.	PUNCT
eurjchem-261	25	1	besides	besides	SCONJ
eurjchem-261	25	2	,	,	PUNCT
eurjchem-261	25	3	the	the	DET
eurjchem-261	25	4	catalyst	catalyst	NOUN
eurjchem-261	25	5	is	be	AUX
eurjchem-261	25	6	inexpensive	inexpensive	ADJ
eurjchem-261	25	7	,	,	PUNCT
eurjchem-261	25	8	basically	basically	ADV
eurjchem-261	25	9	nontoxic	nontoxic	ADJ
eurjchem-261	25	10	,	,	PUNCT
eurjchem-261	25	11	highly	highly	ADV
eurjchem-261	25	12	stable	stable	ADJ
eurjchem-261	25	13	and	and	CCONJ
eurjchem-261	25	14	easily	easily	ADV
eurjchem-261	25	15	available	available	ADJ
eurjchem-261	25	16	.	.	PUNCT
eurjchem-261	26	1	moreover	moreover	ADV
eurjchem-261	26	2	,	,	PUNCT
eurjchem-261	26	3	this	this	DET
eurjchem-261	26	4	method	method	NOUN
eurjchem-261	26	5	is	be	AUX
eurjchem-261	26	6	suitable	suitable	ADJ
eurjchem-261	26	7	for	for	ADP
eurjchem-261	26	8	the	the	DET
eurjchem-261	26	9	synthesis	synthesis	NOUN
eurjchem-261	26	10	of	of	ADP
eurjchem-261	26	11	phosphate	phosphate	ADJ
eurjchem-261	26	12	ester	ester	NOUN
eurjchem-261	26	13	by	by	ADP
eurjchem-261	26	14	using	use	VERB
eurjchem-261	26	15	all	all	DET
eurjchem-261	26	16	the	the	DET
eurjchem-261	26	17	sodium	sodium	NOUN
eurjchem-261	26	18	salts	salt	NOUN
eurjchem-261	26	19	of	of	ADP
eurjchem-261	26	20	dialkyl	dialkyl	PROPN
eurjchem-261	26	21	phosphate	phosphate	NOUN
eurjchem-261	26	22	as	as	ADP
eurjchem-261	26	23	initial	initial	ADJ
eurjchem-261	26	24	material	material	NOUN
eurjchem-261	26	25	,	,	PUNCT
eurjchem-261	26	26	including	include	VERB
eurjchem-261	26	27	sodium	sodium	NOUN
eurjchem-261	26	28	salt	salt	NOUN
eurjchem-261	26	29	of	of	ADP
eurjchem-261	26	30	diethyl	diethyl	NOUN
eurjchem-261	26	31	phosphate	phosphate	NOUN
eurjchem-261	26	32	,	,	PUNCT
eurjchem-261	26	33	the	the	DET
eurjchem-261	26	34	by‐product	by‐product	NOUN
eurjchem-261	26	35	by	by	ADP
eurjchem-261	26	36	employing	employ	VERB
eurjchem-261	26	37	triethyl	triethyl	PROPN
eurjchem-261	26	38	phosphite	phosphite	PROPN
eurjchem-261	26	39	as	as	ADP
eurjchem-261	26	40	catalyst	catalyst	NOUN
eurjchem-261	26	41	in	in	ADP
eurjchem-261	26	42	the	the	DET
eurjchem-261	26	43	basic	basic	ADJ
eurjchem-261	26	44	condition	condition	NOUN
eurjchem-261	26	45	.	.	PUNCT
eurjchem-261	27	1	so	so	ADV
eurjchem-261	27	2	it	it	PRON
eurjchem-261	27	3	is	be	AUX
eurjchem-261	27	4	significant	significant	ADJ
eurjchem-261	27	5	to	to	ADP
eurjchem-261	27	6	this	this	DET
eurjchem-261	27	7	research	research	NOUN
eurjchem-261	27	8	further	far	ADV
eurjchem-261	27	9	.	.	PUNCT
eurjchem-261	28	1	2	2	X
eurjchem-261	28	2	.	.	X
eurjchem-261	28	3	experimental	experimental	ADJ
eurjchem-261	28	4	2.1	2.1	NUM
eurjchem-261	28	5	.	.	PUNCT
eurjchem-261	29	1	instrumentation	instrumentation	NOUN
eurjchem-261	29	2	ir	ir	PROPN
eurjchem-261	29	3	spectrum	spectrum	PROPN
eurjchem-261	29	4	was	be	AUX
eurjchem-261	29	5	prepared	prepare	VERB
eurjchem-261	29	6	on	on	ADP
eurjchem-261	29	7	an	an	DET
eurjchem-261	29	8	alpha	alpha	PROPN
eurjchem-261	29	9	centauri	centauri	PROPN
eurjchem-261	29	10	ft‐ir	ft‐ir	NOUN
eurjchem-261	29	11	spectrometer	spectrometer	NOUN
eurjchem-261	29	12	.	.	PUNCT
eurjchem-261	30	1	1h	1h	NUM
eurjchem-261	30	2	nmr	nmr	NOUN
eurjchem-261	30	3	spectrum	spectrum	NOUN
eurjchem-261	30	4	was	be	AUX
eurjchem-261	30	5	measured	measure	VERB
eurjchem-261	30	6	using	use	VERB
eurjchem-261	30	7	a	a	DET
eurjchem-261	30	8	varian	varian	PROPN
eurjchem-261	30	9	mercury‐300	mercury‐300	ADJ
eurjchem-261	30	10	nmr	nmr	NOUN
eurjchem-261	30	11	spectrometer	spectrometer	NOUN
eurjchem-261	30	12	with	with	ADP
eurjchem-261	30	13	tms	tms	PROPN
eurjchem-261	30	14	as	as	ADP
eurjchem-261	30	15	an	an	DET
eurjchem-261	30	16	internal	internal	ADJ
eurjchem-261	30	17	standard	standard	NOUN
eurjchem-261	30	18	.	.	PUNCT
eurjchem-261	31	1	mass	mass	PROPN
eurjchem-261	31	2	spectra	spectra	PROPN
eurjchem-261	31	3	was	be	AUX
eurjchem-261	31	4	collected	collect	VERB
eurjchem-261	31	5	with	with	ADP
eurjchem-261	31	6	an	an	DET
eurjchem-261	31	7	agilent	agilent	PROPN
eurjchem-261	31	8	5975/6890n	5975/6890n	NUM
eurjchem-261	31	9	gc	gc	PROPN
eurjchem-261	31	10	/	/	SYM
eurjchem-261	31	11	ms	ms	PROPN
eurjchem-261	31	12	spectrometer	spectrometer	NOUN
eurjchem-261	31	13	.	.	PUNCT
eurjchem-261	32	1	thin	thin	ADJ
eurjchem-261	32	2	layer	layer	NOUN
eurjchem-261	32	3	chromatography	chromatography	NOUN
eurjchem-261	32	4	was	be	AUX
eurjchem-261	32	5	carried	carry	VERB
eurjchem-261	32	6	out	out	ADP
eurjchem-261	32	7	on	on	ADP
eurjchem-261	32	8	silica	silica	NOUN
eurjchem-261	32	9	gel	gel	NOUN
eurjchem-261	32	10	gf‐254	gf‐254	NOUN
eurjchem-261	32	11	plates	plate	NOUN
eurjchem-261	32	12	with	with	ADP
eurjchem-261	32	13	petroleum	petroleum	NOUN
eurjchem-261	32	14	ether	ether	NOUN
eurjchem-261	32	15	:	:	PUNCT
eurjchem-261	32	16	ethyl	ethyl	PROPN
eurjchem-261	32	17	acetate	acetate	PROPN
eurjchem-261	32	18	(	(	PUNCT
eurjchem-261	32	19	8:1	8:1	NUM
eurjchem-261	32	20	)	)	PUNCT
eurjchem-261	32	21	as	as	ADP
eurjchem-261	32	22	developing	develop	VERB
eurjchem-261	32	23	agent	agent	NOUN
eurjchem-261	32	24	.	.	PUNCT
eurjchem-261	33	1	refractive	refractive	ADJ
eurjchem-261	33	2	index	index	NOUN
eurjchem-261	33	3	(	(	PUNCT
eurjchem-261	33	4	uncorrected	uncorrecte	VERB
eurjchem-261	33	5	)	)	PUNCT
eurjchem-261	33	6	was	be	AUX
eurjchem-261	33	7	measured	measure	VERB
eurjchem-261	33	8	using	use	VERB
eurjchem-261	33	9	a	a	DET
eurjchem-261	33	10	shanghai	shanghai	PROPN
eurjchem-261	33	11	abbe	abbe	PROPN
eurjchem-261	33	12	refractometer‐2waj	refractometer‐2waj	NOUN
eurjchem-261	33	13	,	,	PUNCT
eurjchem-261	33	14	and	and	CCONJ
eurjchem-261	33	15	compared	compare	VERB
eurjchem-261	33	16	with	with	ADP
eurjchem-261	33	17	the	the	DET
eurjchem-261	33	18	literature	literature	NOUN
eurjchem-261	33	19	value	value	NOUN
eurjchem-261	33	20	.	.	PUNCT
eurjchem-261	34	1	270	270	NUM
eurjchem-261	34	2	ge	ge	PROPN
eurjchem-261	34	3	et	et	PROPN
eurjchem-261	34	4	al	al	PROPN
eurjchem-261	34	5	.	.	PUNCT
eurjchem-261	34	6	/	/	SYM
eurjchem-261	34	7	european	european	PROPN
eurjchem-261	34	8	journal	journal	PROPN
eurjchem-261	34	9	of	of	ADP
eurjchem-261	34	10	chemistry	chemistry	NOUN
eurjchem-261	34	11	2	2	NUM
eurjchem-261	34	12	(	(	PUNCT
eurjchem-261	34	13	2	2	NUM
eurjchem-261	34	14	)	)	PUNCT
eurjchem-261	34	15	(	(	PUNCT
eurjchem-261	34	16	2011	2011	NUM
eurjchem-261	34	17	)	)	PUNCT
eurjchem-261	34	18	269‐271	269‐271	NUM
eurjchem-261	34	19	scheme	scheme	NOUN
eurjchem-261	34	20	1	1	NUM
eurjchem-261	34	21	scheme	scheme	NOUN
eurjchem-261	34	22	2	2	NUM
eurjchem-261	34	23	2.2	2.2	NUM
eurjchem-261	34	24	.	.	PUNCT
eurjchem-261	35	1	materials	material	NOUN
eurjchem-261	35	2	all	all	DET
eurjchem-261	35	3	the	the	DET
eurjchem-261	35	4	reagents	reagent	NOUN
eurjchem-261	35	5	aside	aside	ADV
eurjchem-261	35	6	from	from	ADP
eurjchem-261	35	7	sodium	sodium	NOUN
eurjchem-261	35	8	salt	salt	NOUN
eurjchem-261	35	9	of	of	ADP
eurjchem-261	35	10	diethyl	diethyl	NOUN
eurjchem-261	35	11	phosphate	phosphate	NOUN
eurjchem-261	35	12	were	be	AUX
eurjchem-261	35	13	analytical	analytical	ADJ
eurjchem-261	35	14	pure	pure	ADJ
eurjchem-261	35	15	reagent	reagent	NOUN
eurjchem-261	35	16	and	and	CCONJ
eurjchem-261	35	17	were	be	AUX
eurjchem-261	35	18	used	use	VERB
eurjchem-261	35	19	without	without	ADP
eurjchem-261	35	20	further	further	ADJ
eurjchem-261	35	21	purification	purification	NOUN
eurjchem-261	35	22	.	.	PUNCT
eurjchem-261	36	1	sodium	sodium	NOUN
eurjchem-261	36	2	salt	salt	NOUN
eurjchem-261	36	3	of	of	ADP
eurjchem-261	36	4	diethyl	diethyl	NOUN
eurjchem-261	36	5	phosphate	phosphate	NOUN
eurjchem-261	36	6	derived	derive	VERB
eurjchem-261	36	7	from	from	ADP
eurjchem-261	36	8	the	the	DET
eurjchem-261	36	9	by‐product	by‐product	NOUN
eurjchem-261	36	10	of	of	ADP
eurjchem-261	36	11	fluorescent	fluorescent	ADJ
eurjchem-261	36	12	brightener	brightener	NOUN
eurjchem-261	36	13	er	er	INTJ
eurjchem-261	36	14	in	in	ADP
eurjchem-261	36	15	the	the	DET
eurjchem-261	36	16	factory	factory	NOUN
eurjchem-261	36	17	was	be	AUX
eurjchem-261	36	18	used	use	VERB
eurjchem-261	36	19	with	with	ADP
eurjchem-261	36	20	further	further	ADJ
eurjchem-261	36	21	purification	purification	NOUN
eurjchem-261	36	22	.	.	PUNCT
eurjchem-261	37	1	2.3	2.3	NUM
eurjchem-261	37	2	.	.	PUNCT
eurjchem-261	38	1	synthesis	synthesis	VERB
eurjchem-261	38	2	the	the	DET
eurjchem-261	38	3	optimal	optimal	ADJ
eurjchem-261	38	4	synthesis	synthesis	NOUN
eurjchem-261	38	5	condition	condition	NOUN
eurjchem-261	38	6	is	be	AUX
eurjchem-261	38	7	as	as	SCONJ
eurjchem-261	38	8	follows	follow	VERB
eurjchem-261	38	9	:	:	PUNCT
eurjchem-261	38	10	sodium	sodium	NOUN
eurjchem-261	38	11	salt	salt	NOUN
eurjchem-261	38	12	diethyl	diethyl	NOUN
eurjchem-261	38	13	phosphate	phosphate	NOUN
eurjchem-261	38	14	(	(	PUNCT
eurjchem-261	38	15	0.05	0.05	NUM
eurjchem-261	38	16	mol	mol	NOUN
eurjchem-261	38	17	)	)	PUNCT
eurjchem-261	38	18	,	,	PUNCT
eurjchem-261	38	19	tbab	tbab	PROPN
eurjchem-261	38	20	(	(	PUNCT
eurjchem-261	38	21	0.003	0.003	NUM
eurjchem-261	38	22	mol	mol	NOUN
eurjchem-261	38	23	)	)	PUNCT
eurjchem-261	38	24	,	,	PUNCT
eurjchem-261	38	25	20	20	NUM
eurjchem-261	38	26	ml	ml	NOUN
eurjchem-261	38	27	toluene	toluene	NOUN
eurjchem-261	38	28	and	and	CCONJ
eurjchem-261	38	29	2	2	NUM
eurjchem-261	38	30	ml	ml	NOUN
eurjchem-261	38	31	water	water	NOUN
eurjchem-261	38	32	were	be	AUX
eurjchem-261	38	33	mixed	mix	VERB
eurjchem-261	38	34	in	in	ADP
eurjchem-261	38	35	the	the	DET
eurjchem-261	38	36	three‐neck	three‐neck	NOUN
eurjchem-261	38	37	round‐bottomed	round‐bottomed	ADV
eurjchem-261	38	38	flask	flask	PROPN
eurjchem-261	38	39	.	.	PUNCT
eurjchem-261	39	1	then	then	ADV
eurjchem-261	39	2	benzyl	benzyl	VERB
eurjchem-261	39	3	chloride	chloride	NOUN
eurjchem-261	39	4	(	(	PUNCT
eurjchem-261	39	5	0.05	0.05	NUM
eurjchem-261	39	6	mol	mol	NOUN
eurjchem-261	39	7	)	)	PUNCT
eurjchem-261	39	8	was	be	AUX
eurjchem-261	39	9	added	add	VERB
eurjchem-261	39	10	and	and	CCONJ
eurjchem-261	39	11	stirred	stir	VERB
eurjchem-261	39	12	at	at	ADP
eurjchem-261	39	13	the	the	DET
eurjchem-261	39	14	reflux	reflux	NOUN
eurjchem-261	39	15	temperature	temperature	NOUN
eurjchem-261	39	16	until	until	SCONJ
eurjchem-261	39	17	tlc	tlc	NOUN
eurjchem-261	39	18	analysis	analysis	NOUN
eurjchem-261	39	19	(	(	PUNCT
eurjchem-261	39	20	petroleum	petroleum	NOUN
eurjchem-261	39	21	ether	ether	NOUN
eurjchem-261	39	22	:	:	PUNCT
eurjchem-261	39	23	ethyl	ethyl	PROPN
eurjchem-261	39	24	acetate	acetate	NOUN
eurjchem-261	39	25	,	,	PUNCT
eurjchem-261	39	26	8:1	8:1	NUM
eurjchem-261	39	27	,	,	PUNCT
eurjchem-261	39	28	v	v	NOUN
eurjchem-261	39	29	:	:	SYM
eurjchem-261	39	30	v	v	NOUN
eurjchem-261	39	31	)	)	PUNCT
eurjchem-261	39	32	monitored	monitor	VERB
eurjchem-261	39	33	completion	completion	NOUN
eurjchem-261	39	34	of	of	ADP
eurjchem-261	39	35	the	the	DET
eurjchem-261	39	36	reaction	reaction	NOUN
eurjchem-261	39	37	.	.	PUNCT
eurjchem-261	40	1	then	then	ADV
eurjchem-261	40	2	the	the	DET
eurjchem-261	40	3	mixture	mixture	NOUN
eurjchem-261	40	4	was	be	AUX
eurjchem-261	40	5	cooled	cool	VERB
eurjchem-261	40	6	and	and	CCONJ
eurjchem-261	40	7	poured	pour	VERB
eurjchem-261	40	8	into	into	ADP
eurjchem-261	40	9	toluene	toluene	NOUN
eurjchem-261	40	10	(	(	PUNCT
eurjchem-261	40	11	20	20	NUM
eurjchem-261	40	12	ml	ml	NOUN
eurjchem-261	40	13	)	)	PUNCT
eurjchem-261	40	14	,	,	PUNCT
eurjchem-261	40	15	filtered	filter	VERB
eurjchem-261	40	16	and	and	CCONJ
eurjchem-261	40	17	the	the	DET
eurjchem-261	40	18	residue	residue	NOUN
eurjchem-261	40	19	was	be	AUX
eurjchem-261	40	20	taken	take	VERB
eurjchem-261	40	21	up	up	ADP
eurjchem-261	40	22	in	in	ADP
eurjchem-261	40	23	toluene	toluene	NOUN
eurjchem-261	40	24	.	.	PUNCT
eurjchem-261	41	1	the	the	DET
eurjchem-261	41	2	toluene	toluene	NOUN
eurjchem-261	41	3	layer	layer	NOUN
eurjchem-261	41	4	was	be	AUX
eurjchem-261	41	5	washed	wash	VERB
eurjchem-261	41	6	with	with	ADP
eurjchem-261	41	7	saturated	saturate	VERB
eurjchem-261	41	8	sodium	sodium	NOUN
eurjchem-261	41	9	bicarbonate	bicarbonate	NOUN
eurjchem-261	41	10	(	(	PUNCT
eurjchem-261	41	11	2x15	2x15	NUM
eurjchem-261	41	12	ml	ml	NOUN
eurjchem-261	41	13	)	)	PUNCT
eurjchem-261	41	14	,	,	PUNCT
eurjchem-261	41	15	water	water	NOUN
eurjchem-261	41	16	(	(	PUNCT
eurjchem-261	41	17	2x15	2x15	NUM
eurjchem-261	41	18	ml	ml	NOUN
eurjchem-261	41	19	)	)	PUNCT
eurjchem-261	41	20	,	,	PUNCT
eurjchem-261	41	21	saturated	saturate	VERB
eurjchem-261	41	22	sodium	sodium	NOUN
eurjchem-261	41	23	chloride	chloride	NOUN
eurjchem-261	41	24	(	(	PUNCT
eurjchem-261	41	25	1x20	1x20	NUM
eurjchem-261	41	26	ml	ml	NOUN
eurjchem-261	41	27	)	)	PUNCT
eurjchem-261	41	28	,	,	PUNCT
eurjchem-261	41	29	and	and	CCONJ
eurjchem-261	41	30	dried	dry	VERB
eurjchem-261	41	31	over	over	ADP
eurjchem-261	41	32	anhydrous	anhydrous	ADJ
eurjchem-261	41	33	magnesium	magnesium	NOUN
eurjchem-261	41	34	sulfate	sulfate	NOUN
eurjchem-261	41	35	.	.	PUNCT
eurjchem-261	42	1	after	after	SCONJ
eurjchem-261	42	2	the	the	DET
eurjchem-261	42	3	removal	removal	NOUN
eurjchem-261	42	4	of	of	ADP
eurjchem-261	42	5	the	the	DET
eurjchem-261	42	6	low	low	ADJ
eurjchem-261	42	7	boiling	boiling	NOUN
eurjchem-261	42	8	solvent	solvent	NOUN
eurjchem-261	42	9	,	,	PUNCT
eurjchem-261	42	10	benzyl	benzyl	NOUN
eurjchem-261	42	11	diethyl	diethyl	NOUN
eurjchem-261	42	12	phosphate	phosphate	NOUN
eurjchem-261	42	13	was	be	AUX
eurjchem-261	42	14	collected	collect	VERB
eurjchem-261	42	15	.	.	PUNCT
eurjchem-261	43	1	the	the	DET
eurjchem-261	43	2	benzyl	benzyl	NOUN
eurjchem-261	43	3	diethyl	diethyl	NOUN
eurjchem-261	43	4	phosphate	phosphate	NOUN
eurjchem-261	43	5	was	be	AUX
eurjchem-261	43	6	obtained	obtain	VERB
eurjchem-261	43	7	as	as	ADP
eurjchem-261	43	8	light	light	ADJ
eurjchem-261	43	9	yellow	yellow	ADJ
eurjchem-261	43	10	oil	oil	NOUN
eurjchem-261	43	11	.	.	PUNCT
eurjchem-261	44	1	yield	yield	NOUN
eurjchem-261	44	2	(	(	PUNCT
eurjchem-261	44	3	10.94	10.94	NUM
eurjchem-261	44	4	g	g	NOUN
eurjchem-261	44	5	,	,	PUNCT
eurjchem-261	44	6	89.67	89.67	NUM
eurjchem-261	44	7	%	%	NOUN
eurjchem-261	44	8	)	)	PUNCT
eurjchem-261	44	9	.	.	PUNCT
eurjchem-261	45	1	nd22	nd22	PROPN
eurjchem-261	45	2	1.4895	1.4895	NUM
eurjchem-261	45	3	(	(	PUNCT
eurjchem-261	45	4	lit	lit	ADJ
eurjchem-261	45	5	.	.	PUNCT
eurjchem-261	46	1	[	[	X
eurjchem-261	46	2	16	16	NUM
eurjchem-261	46	3	]	]	X
eurjchem-261	46	4	nd20	nd20	PROPN
eurjchem-261	46	5	1.4846	1.4846	NUM
eurjchem-261	46	6	)	)	PUNCT
eurjchem-261	46	7	.	.	PUNCT
eurjchem-261	47	1	anal	anal	PROPN
eurjchem-261	47	2	.	.	PUNCT
eurjchem-261	47	3	calcd	calcd	NOUN
eurjchem-261	47	4	.	.	PUNCT
eurjchem-261	48	1	for	for	ADP
eurjchem-261	48	2	c11h17po4	c11h17po4	NOUN
eurjchem-261	48	3	:	:	PUNCT
eurjchem-261	48	4	c	c	X
eurjchem-261	48	5	,	,	PUNCT
eurjchem-261	48	6	54.10	54.10	NUM
eurjchem-261	48	7	;	;	PUNCT
eurjchem-261	48	8	h	h	NOUN
eurjchem-261	48	9	,	,	PUNCT
eurjchem-261	48	10	7.02	7.02	NUM
eurjchem-261	48	11	%	%	NOUN
eurjchem-261	48	12	.	.	PUNCT
eurjchem-261	49	1	found	find	VERB
eurjchem-261	49	2	:	:	PUNCT
eurjchem-261	50	1	c	c	X
eurjchem-261	50	2	,	,	PUNCT
eurjchem-261	50	3	54.40	54.40	NUM
eurjchem-261	50	4	;	;	PUNCT
eurjchem-261	50	5	h	h	NOUN
eurjchem-261	50	6	,	,	PUNCT
eurjchem-261	50	7	7.20	7.20	NUM
eurjchem-261	50	8	%	%	NOUN
eurjchem-261	50	9	.	.	PUNCT
eurjchem-261	51	1	ir	ir	PROPN
eurjchem-261	51	2	(	(	PUNCT
eurjchem-261	51	3	νmax	νmax	ADV
eurjchem-261	51	4	,	,	PUNCT
eurjchem-261	51	5	film	film	NOUN
eurjchem-261	51	6	,	,	PUNCT
eurjchem-261	51	7	cm‐1	cm‐1	PROPN
eurjchem-261	51	8	):	):	PUNCT
eurjchem-261	51	9	2983	2983	NUM
eurjchem-261	51	10	,	,	PUNCT
eurjchem-261	51	11	2865	2865	NUM
eurjchem-261	51	12	,	,	PUNCT
eurjchem-261	51	13	1498	1498	NUM
eurjchem-261	51	14	(	(	PUNCT
eurjchem-261	51	15	ch3	ch3	PROPN
eurjchem-261	51	16	)	)	PUNCT
eurjchem-261	51	17	;	;	PUNCT
eurjchem-261	51	18	2933	2933	NUM
eurjchem-261	51	19	,	,	PUNCT
eurjchem-261	51	20	2908	2908	NUM
eurjchem-261	51	21	,	,	PUNCT
eurjchem-261	51	22	2855	2855	NUM
eurjchem-261	51	23	,	,	PUNCT
eurjchem-261	51	24	1456	1456	NUM
eurjchem-261	51	25	(	(	PUNCT
eurjchem-261	51	26	ch2	ch2	PROPN
eurjchem-261	51	27	)	)	PUNCT
eurjchem-261	51	28	;	;	PUNCT
eurjchem-261	51	29	1275	1275	NUM
eurjchem-261	51	30	(	(	PUNCT
eurjchem-261	51	31	p	p	X
eurjchem-261	51	32	=	=	NOUN
eurjchem-261	51	33	o	o	NOUN
eurjchem-261	51	34	)	)	PUNCT
eurjchem-261	51	35	;	;	PUNCT
eurjchem-261	51	36	1034	1034	NUM
eurjchem-261	51	37	,	,	PUNCT
eurjchem-261	51	38	976	976	NUM
eurjchem-261	51	39	(	(	PUNCT
eurjchem-261	51	40	p‐o‐c	p‐o‐c	ADJ
eurjchem-261	51	41	)	)	PUNCT
eurjchem-261	51	42	.	.	PUNCT
eurjchem-261	52	1	1h	1h	NUM
eurjchem-261	52	2	nmr	nmr	NOUN
eurjchem-261	52	3	(	(	PUNCT
eurjchem-261	52	4	300	300	NUM
eurjchem-261	52	5	mhz	mhz	NOUN
eurjchem-261	52	6	;	;	PUNCT
eurjchem-261	52	7	cdcl3	cdcl3	NOUN
eurjchem-261	52	8	,	,	PUNCT
eurjchem-261	52	9	δh	δh	NOUN
eurjchem-261	52	10	):	):	PUNCT
eurjchem-261	52	11	1.28‐1.32	1.28‐1.32	NUM
eurjchem-261	52	12	(	(	PUNCT
eurjchem-261	52	13	t	t	PROPN
eurjchem-261	52	14	,	,	PUNCT
eurjchem-261	52	15	j=7.5	j=7.5	PROPN
eurjchem-261	52	16	hz	hz	PROPN
eurjchem-261	52	17	,	,	PUNCT
eurjchem-261	52	18	6h	6h	NUM
eurjchem-261	52	19	)	)	PUNCT
eurjchem-261	52	20	,	,	PUNCT
eurjchem-261	52	21	4.06‐4.13	4.06‐4.13	NUM
eurjchem-261	52	22	(	(	PUNCT
eurjchem-261	52	23	m	m	PROPN
eurjchem-261	52	24	,	,	PUNCT
eurjchem-261	52	25	j=7.5	j=7.5	PROPN
eurjchem-261	52	26	hz	hz	PROPN
eurjchem-261	52	27	,	,	PUNCT
eurjchem-261	52	28	4h	4h	NOUN
eurjchem-261	52	29	)	)	PUNCT
eurjchem-261	52	30	,	,	PUNCT
eurjchem-261	52	31	5.05‐5.08	5.05‐5.08	NUM
eurjchem-261	52	32	(	(	PUNCT
eurjchem-261	52	33	d	d	NOUN
eurjchem-261	52	34	,	,	PUNCT
eurjchem-261	52	35	j=8.5	j=8.5	PROPN
eurjchem-261	52	36	hz	hz	NOUN
eurjchem-261	52	37	,	,	PUNCT
eurjchem-261	52	38	2h	2h	NUM
eurjchem-261	52	39	)	)	PUNCT
eurjchem-261	52	40	,	,	PUNCT
eurjchem-261	52	41	7.33‐7.39	7.33‐7.39	NUM
eurjchem-261	52	42	(	(	PUNCT
eurjchem-261	52	43	m	m	PROPN
eurjchem-261	52	44	,	,	PUNCT
eurjchem-261	52	45	5h	5h	NUM
eurjchem-261	52	46	)	)	PUNCT
eurjchem-261	52	47	.	.	PUNCT
eurjchem-261	53	1	ms	ms	NOUN
eurjchem-261	53	2	(	(	PUNCT
eurjchem-261	53	3	m	m	PROPN
eurjchem-261	53	4	/	/	SYM
eurjchem-261	53	5	z	z	NOUN
eurjchem-261	53	6	,	,	PUNCT
eurjchem-261	53	7	ir/%	ir/%	NOUN
eurjchem-261	53	8	):	):	PUNCT
eurjchem-261	53	9	246	246	NUM
eurjchem-261	53	10	(	(	PUNCT
eurjchem-261	53	11	2.2	2.2	NUM
eurjchem-261	53	12	)	)	PUNCT
eurjchem-261	53	13	,	,	PUNCT
eurjchem-261	53	14	245	245	NUM
eurjchem-261	53	15	(	(	PUNCT
eurjchem-261	53	16	15.6	15.6	NUM
eurjchem-261	53	17	)	)	PUNCT
eurjchem-261	53	18	,	,	PUNCT
eurjchem-261	53	19	244	244	NUM
eurjchem-261	53	20	(	(	PUNCT
eurjchem-261	53	21	29.2	29.2	NUM
eurjchem-261	53	22	)	)	PUNCT
eurjchem-261	53	23	,	,	PUNCT
eurjchem-261	53	24	215	215	NUM
eurjchem-261	53	25	(	(	PUNCT
eurjchem-261	53	26	15.5	15.5	NUM
eurjchem-261	53	27	)	)	PUNCT
eurjchem-261	53	28	,	,	PUNCT
eurjchem-261	53	29	188	188	NUM
eurjchem-261	53	30	(	(	PUNCT
eurjchem-261	53	31	15.7	15.7	NUM
eurjchem-261	53	32	)	)	PUNCT
eurjchem-261	53	33	,	,	PUNCT
eurjchem-261	53	34	187	187	NUM
eurjchem-261	53	35	(	(	PUNCT
eurjchem-261	53	36	24.7	24.7	NUM
eurjchem-261	53	37	)	)	PUNCT
eurjchem-261	53	38	,	,	PUNCT
eurjchem-261	53	39	153	153	NUM
eurjchem-261	53	40	(	(	PUNCT
eurjchem-261	53	41	10.3	10.3	NUM
eurjchem-261	53	42	)	)	PUNCT
eurjchem-261	53	43	,	,	PUNCT
eurjchem-261	53	44	125	125	NUM
eurjchem-261	53	45	(	(	PUNCT
eurjchem-261	53	46	25.9	25.9	NUM
eurjchem-261	53	47	)	)	PUNCT
eurjchem-261	53	48	,	,	PUNCT
eurjchem-261	53	49	107	107	NUM
eurjchem-261	53	50	(	(	PUNCT
eurjchem-261	53	51	78.6	78.6	NUM
eurjchem-261	53	52	)	)	PUNCT
eurjchem-261	53	53	,	,	PUNCT
eurjchem-261	53	54	91	91	NUM
eurjchem-261	53	55	(	(	PUNCT
eurjchem-261	53	56	100	100	NUM
eurjchem-261	53	57	)	)	PUNCT
eurjchem-261	53	58	.	.	PUNCT
eurjchem-261	54	1	3	3	X
eurjchem-261	54	2	.	.	NOUN
eurjchem-261	54	3	results	result	NOUN
eurjchem-261	54	4	and	and	CCONJ
eurjchem-261	54	5	discussion	discussion	NOUN
eurjchem-261	54	6	a	a	DET
eurjchem-261	54	7	possible	possible	ADJ
eurjchem-261	54	8	mechanism	mechanism	NOUN
eurjchem-261	54	9	for	for	ADP
eurjchem-261	54	10	the	the	DET
eurjchem-261	54	11	reaction	reaction	NOUN
eurjchem-261	54	12	can	can	AUX
eurjchem-261	54	13	be	be	AUX
eurjchem-261	54	14	described	describe	VERB
eurjchem-261	54	15	as	as	ADP
eurjchem-261	54	16	shown	show	VERB
eurjchem-261	54	17	in	in	ADP
eurjchem-261	54	18	scheme	scheme	NOUN
eurjchem-261	54	19	2	2	NUM
eurjchem-261	54	20	,	,	PUNCT
eurjchem-261	54	21	which	which	PRON
eurjchem-261	54	22	involves	involve	VERB
eurjchem-261	54	23	the	the	DET
eurjchem-261	54	24	dissolution	dissolution	NOUN
eurjchem-261	54	25	of	of	ADP
eurjchem-261	54	26	solid	solid	ADJ
eurjchem-261	54	27	(	(	PUNCT
eurjchem-261	54	28	eto)2p(o)o‐	eto)2p(o)o‐	VERB
eurjchem-261	54	29	into	into	ADP
eurjchem-261	54	30	ω‐phase	ω‐phase	NUM
eurjchem-261	54	31	,	,	PUNCT
eurjchem-261	54	32	followed	follow	VERB
eurjchem-261	54	33	by	by	ADP
eurjchem-261	54	34	the	the	DET
eurjchem-261	54	35	anion‐exchange	anion‐exchange	NOUN
eurjchem-261	54	36	reaction	reaction	NOUN
eurjchem-261	54	37	with	with	ADP
eurjchem-261	54	38	the	the	DET
eurjchem-261	54	39	quaternary	quaternary	ADJ
eurjchem-261	54	40	ammonium	ammonium	NOUN
eurjchem-261	54	41	salt	salt	NOUN
eurjchem-261	54	42	q+x‐	q+x‐	VERB
eurjchem-261	54	43	to	to	PART
eurjchem-261	54	44	form	form	VERB
eurjchem-261	54	45	the	the	DET
eurjchem-261	54	46	active	active	ADJ
eurjchem-261	54	47	ion	ion	NOUN
eurjchem-261	54	48	pair	pair	NOUN
eurjchem-261	54	49	(	(	PUNCT
eurjchem-261	54	50	eto)2p(o)o‐q+	eto)2p(o)o‐q+	X
eurjchem-261	54	51	in	in	ADP
eurjchem-261	54	52	the	the	DET
eurjchem-261	54	53	ω‐phase	ω‐phase	NOUN
eurjchem-261	54	54	,	,	PUNCT
eurjchem-261	54	55	a	a	DET
eurjchem-261	54	56	layer	layer	NOUN
eurjchem-261	54	57	around	around	ADP
eurjchem-261	54	58	the	the	DET
eurjchem-261	54	59	solid	solid	ADJ
eurjchem-261	54	60	phase	phase	NOUN
eurjchem-261	54	61	and	and	CCONJ
eurjchem-261	54	62	organic	organic	ADJ
eurjchem-261	54	63	phase	phase	NOUN
eurjchem-261	54	64	,	,	PUNCT
eurjchem-261	54	65	then	then	ADV
eurjchem-261	54	66	(	(	PUNCT
eurjchem-261	54	67	eto)2p(o)o‐q+	eto)2p(o)o‐q+	X
eurjchem-261	54	68	is	be	AUX
eurjchem-261	54	69	transferred	transfer	VERB
eurjchem-261	54	70	to	to	ADP
eurjchem-261	54	71	the	the	DET
eurjchem-261	54	72	organic	organic	ADJ
eurjchem-261	54	73	phase	phase	NOUN
eurjchem-261	54	74	,	,	PUNCT
eurjchem-261	54	75	where	where	SCONJ
eurjchem-261	54	76	the	the	DET
eurjchem-261	54	77	diethyl	diethyl	NOUN
eurjchem-261	54	78	phosphate	phosphate	NOUN
eurjchem-261	54	79	anion	anion	NOUN
eurjchem-261	54	80	substitution	substitution	NOUN
eurjchem-261	54	81	on	on	ADP
eurjchem-261	54	82	benzyl	benzyl	NOUN
eurjchem-261	54	83	chloride	chloride	NOUN
eurjchem-261	54	84	takes	take	VERB
eurjchem-261	54	85	place	place	NOUN
eurjchem-261	54	86	.	.	PUNCT
eurjchem-261	55	1	addition	addition	NOUN
eurjchem-261	55	2	of	of	ADP
eurjchem-261	55	3	small	small	ADJ
eurjchem-261	55	4	quantities	quantity	NOUN
eurjchem-261	55	5	of	of	ADP
eurjchem-261	55	6	water	water	NOUN
eurjchem-261	55	7	also	also	ADV
eurjchem-261	55	8	facilitates	facilitate	VERB
eurjchem-261	55	9	the	the	DET
eurjchem-261	55	10	distribution	distribution	NOUN
eurjchem-261	55	11	of	of	ADP
eurjchem-261	55	12	the	the	DET
eurjchem-261	55	13	quaternary	quaternary	ADJ
eurjchem-261	55	14	salt	salt	NOUN
eurjchem-261	55	15	between	between	ADP
eurjchem-261	55	16	the	the	DET
eurjchem-261	55	17	organic	organic	ADJ
eurjchem-261	55	18	phase	phase	NOUN
eurjchem-261	55	19	and	and	CCONJ
eurjchem-261	55	20	solid	solid	ADJ
eurjchem-261	55	21	phase	phase	NOUN
eurjchem-261	55	22	(	(	PUNCT
eurjchem-261	55	23	scheme	scheme	NOUN
eurjchem-261	55	24	2	2	NUM
eurjchem-261	55	25	)	)	PUNCT
eurjchem-261	55	26	.	.	PUNCT
eurjchem-261	56	1	to	to	PART
eurjchem-261	56	2	obtain	obtain	VERB
eurjchem-261	56	3	the	the	DET
eurjchem-261	56	4	high	high	ADJ
eurjchem-261	56	5	yield	yield	NOUN
eurjchem-261	56	6	,	,	PUNCT
eurjchem-261	56	7	we	we	PRON
eurjchem-261	56	8	attempted	attempt	VERB
eurjchem-261	56	9	to	to	PART
eurjchem-261	56	10	optimize	optimize	VERB
eurjchem-261	56	11	the	the	DET
eurjchem-261	56	12	reaction	reaction	NOUN
eurjchem-261	56	13	conditions	condition	NOUN
eurjchem-261	56	14	on	on	ADP
eurjchem-261	56	15	the	the	DET
eurjchem-261	56	16	different	different	ADJ
eurjchem-261	56	17	phase	phase	NOUN
eurjchem-261	56	18	transfer	transfer	NOUN
eurjchem-261	56	19	catalysts	catalyst	NOUN
eurjchem-261	56	20	.	.	PUNCT
eurjchem-261	57	1	the	the	DET
eurjchem-261	57	2	results	result	NOUN
eurjchem-261	57	3	were	be	AUX
eurjchem-261	57	4	as	as	ADP
eurjchem-261	57	5	shown	show	VERB
eurjchem-261	57	6	in	in	ADP
eurjchem-261	57	7	table	table	NOUN
eurjchem-261	57	8	1	1	NUM
eurjchem-261	57	9	,	,	PUNCT
eurjchem-261	57	10	triethyl	triethyl	NOUN
eurjchem-261	57	11	benzyl	benzyl	NOUN
eurjchem-261	57	12	ammonium	ammonium	NOUN
eurjchem-261	57	13	chloride	chloride	NOUN
eurjchem-261	57	14	(	(	PUNCT
eurjchem-261	57	15	teba	teba	NOUN
eurjchem-261	57	16	)	)	PUNCT
eurjchem-261	57	17	,	,	PUNCT
eurjchem-261	57	18	cetyl	cetyl	NOUN
eurjchem-261	57	19	trimethyl	trimethyl	NOUN
eurjchem-261	57	20	ammonium	ammonium	NOUN
eurjchem-261	57	21	bromide	bromide	NOUN
eurjchem-261	57	22	(	(	PUNCT
eurjchem-261	57	23	ctab	ctab	NOUN
eurjchem-261	57	24	)	)	PUNCT
eurjchem-261	57	25	,	,	PUNCT
eurjchem-261	57	26	and	and	CCONJ
eurjchem-261	57	27	polyethylene	polyethylene	NOUN
eurjchem-261	57	28	glycol‐400	glycol‐400	NOUN
eurjchem-261	57	29	(	(	PUNCT
eurjchem-261	57	30	peg‐400	peg‐400	NOUN
eurjchem-261	57	31	)	)	PUNCT
eurjchem-261	57	32	to	to	PART
eurjchem-261	57	33	be	be	AUX
eurjchem-261	57	34	less	less	ADV
eurjchem-261	57	35	effective	effective	ADJ
eurjchem-261	57	36	than	than	ADP
eurjchem-261	57	37	tbab	tbab	PROPN
eurjchem-261	57	38	in	in	ADP
eurjchem-261	57	39	our	our	PRON
eurjchem-261	57	40	laboratory	laboratory	NOUN
eurjchem-261	57	41	(	(	PUNCT
eurjchem-261	57	42	entries	entry	NOUN
eurjchem-261	57	43	1‐4	1‐4	NOUN
eurjchem-261	57	44	)	)	PUNCT
eurjchem-261	57	45	.	.	PUNCT
eurjchem-261	58	1	this	this	PRON
eurjchem-261	58	2	is	be	AUX
eurjchem-261	58	3	because	because	SCONJ
eurjchem-261	58	4	the	the	DET
eurjchem-261	58	5	catalyst	catalyst	NOUN
eurjchem-261	58	6	tbab	tbab	NOUN
eurjchem-261	58	7	cation	cation	NOUN
eurjchem-261	58	8	q+	q+	PUNCT
eurjchem-261	58	9	possess	possess	VERB
eurjchem-261	58	10	the	the	DET
eurjchem-261	58	11	better	well	ADJ
eurjchem-261	58	12	distribution	distribution	NOUN
eurjchem-261	58	13	in	in	ADP
eurjchem-261	58	14	the	the	DET
eurjchem-261	58	15	organic	organic	ADJ
eurjchem-261	58	16	phase	phase	NOUN
eurjchem-261	58	17	,	,	PUNCT
eurjchem-261	58	18	(	(	PUNCT
eurjchem-261	58	19	eto)2p(o)o‐	eto)2p(o)o‐	PRON
eurjchem-261	58	20	could	could	AUX
eurjchem-261	58	21	efficiently	efficiently	ADV
eurjchem-261	58	22	be	be	AUX
eurjchem-261	58	23	transferred	transfer	VERB
eurjchem-261	58	24	to	to	ADP
eurjchem-261	58	25	the	the	DET
eurjchem-261	58	26	organic	organic	ADJ
eurjchem-261	58	27	phase	phase	NOUN
eurjchem-261	58	28	by	by	ADP
eurjchem-261	58	29	q+	q+	ADV
eurjchem-261	58	30	,	,	PUNCT
eurjchem-261	58	31	further	far	ADV
eurjchem-261	58	32	enhanced	enhance	VERB
eurjchem-261	58	33	the	the	DET
eurjchem-261	58	34	nucleophilic	nucleophilic	ADJ
eurjchem-261	58	35	property	property	NOUN
eurjchem-261	58	36	of	of	ADP
eurjchem-261	58	37	(	(	PUNCT
eurjchem-261	58	38	eto)2p(o)o‐.	eto)2p(o)o‐.	PROPN
eurjchem-261	58	39	the	the	DET
eurjchem-261	58	40	results	result	NOUN
eurjchem-261	58	41	were	be	AUX
eurjchem-261	58	42	in	in	ADP
eurjchem-261	58	43	agreement	agreement	NOUN
eurjchem-261	58	44	with	with	ADP
eurjchem-261	58	45	the	the	DET
eurjchem-261	58	46	published	publish	VERB
eurjchem-261	58	47	literature	literature	NOUN
eurjchem-261	58	48	[	[	X
eurjchem-261	58	49	17‐20	17‐20	X
eurjchem-261	58	50	]	]	X
eurjchem-261	58	51	.	.	PUNCT
eurjchem-261	59	1	to	to	PART
eurjchem-261	59	2	adequately	adequately	ADV
eurjchem-261	59	3	utilize	utilize	VERB
eurjchem-261	59	4	the	the	DET
eurjchem-261	59	5	side‐product	side‐product	NOUN
eurjchem-261	59	6	of	of	ADP
eurjchem-261	59	7	industrial	industrial	ADJ
eurjchem-261	59	8	products	product	NOUN
eurjchem-261	59	9	sodium	sodium	NOUN
eurjchem-261	59	10	salt	salt	NOUN
eurjchem-261	59	11	of	of	ADP
eurjchem-261	59	12	diethyl	diethyl	NOUN
eurjchem-261	59	13	phosphate	phosphate	NOUN
eurjchem-261	59	14	,	,	PUNCT
eurjchem-261	59	15	the	the	DET
eurjchem-261	59	16	effect	effect	NOUN
eurjchem-261	59	17	of	of	ADP
eurjchem-261	59	18	molar	molar	ADJ
eurjchem-261	59	19	ratios	ratio	NOUN
eurjchem-261	59	20	of	of	ADP
eurjchem-261	59	21	sodium	sodium	NOUN
eurjchem-261	59	22	salt	salt	NOUN
eurjchem-261	59	23	of	of	ADP
eurjchem-261	59	24	diethyl	diethyl	NOUN
eurjchem-261	59	25	phosphate	phosphate	NOUN
eurjchem-261	59	26	to	to	PART
eurjchem-261	59	27	benzyl	benzyl	VERB
eurjchem-261	59	28	chloride	chloride	NOUN
eurjchem-261	59	29	were	be	AUX
eurjchem-261	59	30	studied	study	VERB
eurjchem-261	59	31	for	for	ADP
eurjchem-261	59	32	1:1	1:1	NUM
eurjchem-261	59	33	,	,	PUNCT
eurjchem-261	59	34	1:1.2	1:1.2	NUM
eurjchem-261	59	35	,	,	PUNCT
eurjchem-261	59	36	1:1.5	1:1.5	NUM
eurjchem-261	59	37	,	,	PUNCT
eurjchem-261	59	38	and	and	CCONJ
eurjchem-261	59	39	1:2	1:2	NUM
eurjchem-261	59	40	under	under	ADP
eurjchem-261	59	41	otherwise	otherwise	ADV
eurjchem-261	59	42	similar	similar	ADJ
eurjchem-261	59	43	conditions	condition	NOUN
eurjchem-261	59	44	(	(	PUNCT
eurjchem-261	59	45	entries	entry	NOUN
eurjchem-261	59	46	4	4	NUM
eurjchem-261	59	47	,	,	PUNCT
eurjchem-261	59	48	10‐12	10‐12	NUM
eurjchem-261	59	49	)	)	PUNCT
eurjchem-261	59	50	.	.	PUNCT
eurjchem-261	60	1	the	the	DET
eurjchem-261	60	2	yield	yield	NOUN
eurjchem-261	60	3	of	of	ADP
eurjchem-261	60	4	the	the	DET
eurjchem-261	60	5	product	product	NOUN
eurjchem-261	60	6	was	be	AUX
eurjchem-261	60	7	not	not	PART
eurjchem-261	60	8	obviously	obviously	ADV
eurjchem-261	60	9	enhanced	enhance	VERB
eurjchem-261	60	10	with	with	ADP
eurjchem-261	60	11	the	the	DET
eurjchem-261	60	12	use	use	NOUN
eurjchem-261	60	13	of	of	ADP
eurjchem-261	60	14	higher	high	ADJ
eurjchem-261	60	15	concentration	concentration	NOUN
eurjchem-261	60	16	of	of	ADP
eurjchem-261	60	17	the	the	DET
eurjchem-261	60	18	tbab	tbab	NOUN
eurjchem-261	60	19	catalyst	catalyst	NOUN
eurjchem-261	60	20	(	(	PUNCT
eurjchem-261	60	21	up	up	ADP
eurjchem-261	60	22	to	to	PART
eurjchem-261	60	23	8	8	NUM
eurjchem-261	60	24	mol%	mol%	NOUN
eurjchem-261	60	25	,	,	PUNCT
eurjchem-261	60	26	based	base	VERB
eurjchem-261	60	27	on	on	ADP
eurjchem-261	60	28	the	the	DET
eurjchem-261	60	29	sodium	sodium	NOUN
eurjchem-261	60	30	salt	salt	NOUN
eurjchem-261	60	31	of	of	ADP
eurjchem-261	60	32	diethyl	diethyl	NOUN
eurjchem-261	60	33	phosphate	phosphate	NOUN
eurjchem-261	60	34	,	,	PUNCT
eurjchem-261	60	35	entries	entry	NOUN
eurjchem-261	60	36	4‐9	4‐9	NOUN
eurjchem-261	60	37	)	)	PUNCT
eurjchem-261	60	38	and	and	CCONJ
eurjchem-261	60	39	a	a	DET
eurjchem-261	60	40	1.2~2.0	1.2~2.0	NUM
eurjchem-261	60	41	times	time	NOUN
eurjchem-261	60	42	excess	excess	ADJ
eurjchem-261	60	43	benzyl	benzyl	NOUN
eurjchem-261	60	44	chloride	chloride	NOUN
eurjchem-261	60	45	(	(	PUNCT
eurjchem-261	60	46	entries	entry	NOUN
eurjchem-261	60	47	10‐	10‐	NUM
eurjchem-261	60	48	12	12	NUM
eurjchem-261	60	49	)	)	PUNCT
eurjchem-261	60	50	,	,	PUNCT
eurjchem-261	60	51	due	due	ADP
eurjchem-261	60	52	to	to	ADP
eurjchem-261	60	53	the	the	DET
eurjchem-261	60	54	fact	fact	NOUN
eurjchem-261	60	55	that	that	SCONJ
eurjchem-261	60	56	the	the	DET
eurjchem-261	60	57	concentration	concentration	NOUN
eurjchem-261	60	58	of	of	ADP
eurjchem-261	60	59	(	(	PUNCT
eurjchem-261	60	60	eto)2p(o)o‐q+	eto)2p(o)o‐q+	PUNCT
eurjchem-261	60	61	extracted	extract	VERB
eurjchem-261	60	62	into	into	ADP
eurjchem-261	60	63	the	the	PRON
eurjchem-261	60	64	ω‐phase	ω‐phase	NUM
eurjchem-261	60	65	retains	retain	VERB
eurjchem-261	60	66	almost	almost	ADV
eurjchem-261	60	67	constant	constant	ADJ
eurjchem-261	60	68	with	with	ADP
eurjchem-261	60	69	the	the	DET
eurjchem-261	60	70	ion‐exchange	ion‐exchange	NOUN
eurjchem-261	60	71	reaction	reaction	NOUN
eurjchem-261	60	72	proceeding	proceeding	NOUN
eurjchem-261	60	73	.	.	PUNCT
eurjchem-261	61	1	this	this	DET
eurjchem-261	61	2	phenomenon	phenomenon	NOUN
eurjchem-261	61	3	is	be	AUX
eurjchem-261	61	4	also	also	ADV
eurjchem-261	61	5	observed	observe	VERB
eurjchem-261	61	6	in	in	ADP
eurjchem-261	61	7	most	most	ADJ
eurjchem-261	61	8	other	other	ADJ
eurjchem-261	61	9	solid‐liquid	solid‐liquid	ADJ
eurjchem-261	61	10	phase	phase	NOUN
eurjchem-261	61	11	transfer	transfer	NOUN
eurjchem-261	61	12	catalyzed	catalyze	VERB
eurjchem-261	61	13	reactions	reaction	NOUN
eurjchem-261	61	14	[	[	X
eurjchem-261	61	15	21,22	21,22	X
eurjchem-261	61	16	]	]	X
eurjchem-261	61	17	.	.	PUNCT
eurjchem-261	62	1	furthermore	furthermore	ADV
eurjchem-261	62	2	,	,	PUNCT
eurjchem-261	62	3	considering	consider	VERB
eurjchem-261	62	4	the	the	DET
eurjchem-261	62	5	cost	cost	NOUN
eurjchem-261	62	6	of	of	ADP
eurjchem-261	62	7	consumed	consume	VERB
eurjchem-261	62	8	materials	material	NOUN
eurjchem-261	62	9	,	,	PUNCT
eurjchem-261	62	10	6	6	NUM
eurjchem-261	62	11	mol%	mol%	NOUN
eurjchem-261	62	12	of	of	ADP
eurjchem-261	62	13	tbab	tbab	PROPN
eurjchem-261	62	14	and	and	CCONJ
eurjchem-261	62	15	the	the	DET
eurjchem-261	62	16	molar	molar	ADJ
eurjchem-261	62	17	ratio	ratio	NOUN
eurjchem-261	62	18	1:1	1:1	NUM
eurjchem-261	62	19	of	of	ADP
eurjchem-261	62	20	sodium	sodium	NOUN
eurjchem-261	62	21	salt	salt	NOUN
eurjchem-261	62	22	of	of	ADP
eurjchem-261	62	23	diethyl	diethyl	NOUN
eurjchem-261	62	24	phosphate	phosphate	NOUN
eurjchem-261	62	25	to	to	PART
eurjchem-261	62	26	benzyl	benzyl	VERB
eurjchem-261	62	27	chloride	chloride	NOUN
eurjchem-261	62	28	was	be	AUX
eurjchem-261	62	29	taken	take	VERB
eurjchem-261	62	30	for	for	ADP
eurjchem-261	62	31	all	all	DET
eurjchem-261	62	32	the	the	DET
eurjchem-261	62	33	reactions	reaction	NOUN
eurjchem-261	62	34	.	.	PUNCT
eurjchem-261	63	1	however	however	ADV
eurjchem-261	63	2	,	,	PUNCT
eurjchem-261	63	3	surprisingly	surprisingly	ADV
eurjchem-261	63	4	,	,	PUNCT
eurjchem-261	63	5	the	the	DET
eurjchem-261	63	6	yield	yield	NOUN
eurjchem-261	63	7	of	of	ADP
eurjchem-261	63	8	the	the	DET
eurjchem-261	63	9	product	product	NOUN
eurjchem-261	63	10	was	be	AUX
eurjchem-261	63	11	notably	notably	ADV
eurjchem-261	63	12	enhanced	enhance	VERB
eurjchem-261	63	13	when	when	SCONJ
eurjchem-261	63	14	a	a	DET
eurjchem-261	63	15	little	little	ADJ
eurjchem-261	63	16	water	water	NOUN
eurjchem-261	63	17	was	be	AUX
eurjchem-261	63	18	introduced	introduce	VERB
eurjchem-261	63	19	.	.	PUNCT
eurjchem-261	64	1	in	in	ADP
eurjchem-261	64	2	the	the	DET
eurjchem-261	64	3	present	present	ADJ
eurjchem-261	64	4	study	study	NOUN
eurjchem-261	64	5	,	,	PUNCT
eurjchem-261	64	6	the	the	DET
eurjchem-261	64	7	effect	effect	NOUN
eurjchem-261	64	8	of	of	ADP
eurjchem-261	64	9	the	the	DET
eurjchem-261	64	10	amount	amount	NOUN
eurjchem-261	64	11	of	of	ADP
eurjchem-261	64	12	water	water	NOUN
eurjchem-261	64	13	on	on	ADP
eurjchem-261	64	14	yields	yield	NOUN
eurjchem-261	64	15	was	be	AUX
eurjchem-261	64	16	also	also	ADV
eurjchem-261	64	17	investigated	investigate	VERB
eurjchem-261	64	18	(	(	PUNCT
eurjchem-261	64	19	entries	entry	NOUN
eurjchem-261	64	20	4	4	NUM
eurjchem-261	64	21	,	,	PUNCT
eurjchem-261	64	22	13‐16	13‐16	NUM
eurjchem-261	64	23	)	)	PUNCT
eurjchem-261	64	24	.	.	PUNCT
eurjchem-261	65	1	previous	previous	ADJ
eurjchem-261	65	2	literature	literature	NOUN
eurjchem-261	65	3	generally	generally	ADV
eurjchem-261	65	4	indicated	indicate	VERB
eurjchem-261	65	5	that	that	SCONJ
eurjchem-261	65	6	adding	add	VERB
eurjchem-261	65	7	a	a	DET
eurjchem-261	65	8	little	little	ADJ
eurjchem-261	65	9	water	water	NOUN
eurjchem-261	65	10	to	to	PART
eurjchem-261	65	11	form	form	VERB
eurjchem-261	65	12	the	the	DET
eurjchem-261	65	13	ω‐phase	ω‐phase	NUM
eurjchem-261	65	14	,	,	PUNCT
eurjchem-261	65	15	which	which	PRON
eurjchem-261	65	16	would	would	AUX
eurjchem-261	65	17	enhance	enhance	VERB
eurjchem-261	65	18	the	the	DET
eurjchem-261	65	19	rate	rate	NOUN
eurjchem-261	65	20	of	of	ADP
eurjchem-261	65	21	the	the	DET
eurjchem-261	65	22	reaction	reaction	NOUN
eurjchem-261	65	23	[	[	X
eurjchem-261	65	24	23	23	NUM
eurjchem-261	65	25	]	]	PUNCT
eurjchem-261	65	26	.	.	PUNCT
eurjchem-261	66	1	for	for	ADP
eurjchem-261	66	2	clarity	clarity	NOUN
eurjchem-261	66	3	,	,	PUNCT
eurjchem-261	66	4	it	it	PRON
eurjchem-261	66	5	was	be	AUX
eurjchem-261	66	6	observed	observe	VERB
eurjchem-261	66	7	that	that	SCONJ
eurjchem-261	66	8	small	small	ADJ
eurjchem-261	66	9	quantities	quantity	NOUN
eurjchem-261	66	10	of	of	ADP
eurjchem-261	66	11	water	water	NOUN
eurjchem-261	66	12	(	(	PUNCT
eurjchem-261	66	13	1	1	NUM
eurjchem-261	66	14	ml	ml	NOUN
eurjchem-261	66	15	or	or	CCONJ
eurjchem-261	66	16	2	2	NUM
eurjchem-261	66	17	ml	ml	NOUN
eurjchem-261	66	18	)	)	PUNCT
eurjchem-261	66	19	substantially	substantially	ADV
eurjchem-261	66	20	increase	increase	VERB
eurjchem-261	66	21	the	the	DET
eurjchem-261	66	22	yield	yield	NOUN
eurjchem-261	66	23	and	and	CCONJ
eurjchem-261	66	24	purity	purity	NOUN
eurjchem-261	66	25	of	of	ADP
eurjchem-261	66	26	product	product	NOUN
eurjchem-261	66	27	compared	compare	VERB
eurjchem-261	66	28	to	to	ADP
eurjchem-261	66	29	those	those	PRON
eurjchem-261	66	30	under	under	ADP
eurjchem-261	66	31	adding	add	VERB
eurjchem-261	66	32	more	more	ADJ
eurjchem-261	66	33	water	water	NOUN
eurjchem-261	66	34	above	above	ADP
eurjchem-261	66	35	5ml	5ml	NOUN
eurjchem-261	66	36	.	.	PUNCT
eurjchem-261	67	1	ge	ge	PROPN
eurjchem-261	67	2	et	et	PROPN
eurjchem-261	67	3	al	al	PROPN
eurjchem-261	67	4	.	.	PUNCT
eurjchem-261	67	5	/	/	SYM
eurjchem-261	67	6	european	european	PROPN
eurjchem-261	67	7	journal	journal	PROPN
eurjchem-261	67	8	of	of	ADP
eurjchem-261	67	9	chemistry	chemistry	NOUN
eurjchem-261	67	10	2	2	NUM
eurjchem-261	67	11	(	(	PUNCT
eurjchem-261	67	12	2	2	NUM
eurjchem-261	67	13	)	)	PUNCT
eurjchem-261	67	14	(	(	PUNCT
eurjchem-261	67	15	2011	2011	NUM
eurjchem-261	67	16	)	)	PUNCT
eurjchem-261	67	17	269‐271	269‐271	NOUN
eurjchem-261	67	18	271	271	NUM
eurjchem-261	67	19	table	table	NOUN
eurjchem-261	67	20	1	1	NUM
eurjchem-261	67	21	.	.	PUNCT
eurjchem-261	68	1	preparation	preparation	NOUN
eurjchem-261	68	2	of	of	ADP
eurjchem-261	68	3	benzyl	benzyl	NOUN
eurjchem-261	68	4	diethyl	diethyl	NOUN
eurjchem-261	68	5	phosphate	phosphate	NOUN
eurjchem-261	68	6	from	from	ADP
eurjchem-261	68	7	sodium	sodium	NOUN
eurjchem-261	68	8	salt	salt	NOUN
eurjchem-261	68	9	of	of	ADP
eurjchem-261	68	10	diethyl	diethyl	NOUN
eurjchem-261	68	11	phosphate	phosphate	NOUN
eurjchem-261	68	12	and	and	CCONJ
eurjchem-261	68	13	benzyl	benzyl	NOUN
eurjchem-261	68	14	chloride	chloride	NOUN
eurjchem-261	68	15	under	under	ADP
eurjchem-261	68	16	various	various	ADJ
eurjchem-261	68	17	conditionsa	conditionsa	NOUN
eurjchem-261	68	18	.	.	PUNCT
eurjchem-261	69	1	entries	entry	NOUN
eurjchem-261	69	2	raw	raw	ADJ
eurjchem-261	69	3	material	material	NOUN
eurjchem-261	69	4	ratio	ratio	PROPN
eurjchem-261	69	5	b	b	PROPN
eurjchem-261	69	6	ptc	ptc	PROPN
eurjchem-261	69	7	(	(	PUNCT
eurjchem-261	69	8	%	%	NOUN
eurjchem-261	69	9	mol	mol	NOUN
eurjchem-261	69	10	)	)	PUNCT
eurjchem-261	69	11	c	c	NOUN
eurjchem-261	69	12	solvent	solvent	NOUN
eurjchem-261	69	13	toluene	toluene	NOUN
eurjchem-261	69	14	/	/	SYM
eurjchem-261	69	15	water	water	NOUN
eurjchem-261	69	16	(	(	PUNCT
eurjchem-261	69	17	ml	ml	NOUN
eurjchem-261	69	18	/	/	SYM
eurjchem-261	69	19	ml	ml	NOUN
eurjchem-261	69	20	)	)	PUNCT
eurjchem-261	69	21	temperature	temperature	NOUN
eurjchem-261	69	22	(	(	PUNCT
eurjchem-261	69	23	oc	oc	NOUN
eurjchem-261	69	24	)	)	PUNCT
eurjchem-261	69	25	yield	yield	NOUN
eurjchem-261	69	26	d	d	PROPN
eurjchem-261	69	27	,	,	PUNCT
eurjchem-261	69	28	e	e	NOUN
eurjchem-261	69	29	(	(	PUNCT
eurjchem-261	69	30	%	%	INTJ
eurjchem-261	69	31	)	)	PUNCT
eurjchem-261	70	1	1	1	NUM
eurjchem-261	70	2	1:1	1:1	NUM
eurjchem-261	70	3	6	6	NUM
eurjchem-261	70	4	%	%	NOUN
eurjchem-261	70	5	ctab	ctab	NOUN
eurjchem-261	70	6	20/3	20/3	NUM
eurjchem-261	70	7	reflux	reflux	NOUN
eurjchem-261	70	8	38.44	38.44	NUM
eurjchem-261	70	9	2	2	NUM
eurjchem-261	70	10	1:1	1:1	NUM
eurjchem-261	70	11	6	6	NUM
eurjchem-261	70	12	%	%	NOUN
eurjchem-261	70	13	teba	teba	NOUN
eurjchem-261	71	1	20/3	20/3	NUM
eurjchem-261	71	2	reflux	reflux	NOUN
eurjchem-261	71	3	23.60	23.60	NUM
eurjchem-261	71	4	3	3	NUM
eurjchem-261	71	5	1:1	1:1	NUM
eurjchem-261	71	6	6	6	NUM
eurjchem-261	71	7	%	%	NOUN
eurjchem-261	71	8	peg‐400	peg‐400	NOUN
eurjchem-261	71	9	20/3	20/3	NUM
eurjchem-261	71	10	reflux	reflux	NOUN
eurjchem-261	71	11	11.15	11.15	NUM
eurjchem-261	71	12	4	4	NUM
eurjchem-261	71	13	1:1	1:1	NUM
eurjchem-261	71	14	6	6	NUM
eurjchem-261	71	15	%	%	NOUN
eurjchem-261	71	16	tbab	tbab	NOUN
eurjchem-261	71	17	20/3	20/3	NUM
eurjchem-261	71	18	reflux	reflux	VERB
eurjchem-261	71	19	64.30	64.30	NUM
eurjchem-261	71	20	5	5	NUM
eurjchem-261	71	21	1:1	1:1	NUM
eurjchem-261	71	22	3	3	NUM
eurjchem-261	71	23	%	%	NOUN
eurjchem-261	71	24	tbab	tbab	NOUN
eurjchem-261	71	25	20/3	20/3	NUM
eurjchem-261	71	26	reflux	reflux	VERB
eurjchem-261	71	27	42.70	42.70	NUM
eurjchem-261	71	28	6	6	NUM
eurjchem-261	71	29	1:1	1:1	NUM
eurjchem-261	71	30	4	4	NUM
eurjchem-261	71	31	%	%	NOUN
eurjchem-261	71	32	tbab	tbab	NOUN
eurjchem-261	71	33	20/3	20/3	NUM
eurjchem-261	71	34	reflux	reflux	VERB
eurjchem-261	71	35	50.90	50.90	NUM
eurjchem-261	71	36	7	7	NUM
eurjchem-261	71	37	1:1	1:1	NUM
eurjchem-261	71	38	5	5	NUM
eurjchem-261	71	39	%	%	NOUN
eurjchem-261	71	40	tbab	tbab	NOUN
eurjchem-261	72	1	20/3	20/3	NUM
eurjchem-261	72	2	reflux	reflux	VERB
eurjchem-261	72	3	59.84	59.84	NUM
eurjchem-261	72	4	8	8	NUM
eurjchem-261	72	5	1:1	1:1	NUM
eurjchem-261	72	6	7	7	NUM
eurjchem-261	72	7	%	%	NOUN
eurjchem-261	72	8	tbab	tbab	NOUN
eurjchem-261	72	9	20/3	20/3	NUM
eurjchem-261	72	10	reflux	reflux	VERB
eurjchem-261	72	11	67.54	67.54	NUM
eurjchem-261	72	12	9	9	NUM
eurjchem-261	72	13	1:1	1:1	NUM
eurjchem-261	72	14	8	8	NUM
eurjchem-261	72	15	%	%	NOUN
eurjchem-261	72	16	tbab	tbab	NOUN
eurjchem-261	72	17	20/3	20/3	NUM
eurjchem-261	72	18	reflux	reflux	VERB
eurjchem-261	72	19	69.15	69.15	NUM
eurjchem-261	72	20	10	10	NUM
eurjchem-261	72	21	1:1.2	1:1.2	NUM
eurjchem-261	72	22	6	6	NUM
eurjchem-261	72	23	%	%	NOUN
eurjchem-261	72	24	tbab	tbab	NOUN
eurjchem-261	73	1	20/3	20/3	NUM
eurjchem-261	73	2	reflux	reflux	VERB
eurjchem-261	73	3	65.24	65.24	NUM
eurjchem-261	73	4	11	11	NUM
eurjchem-261	73	5	1:1.5	1:1.5	NUM
eurjchem-261	73	6	6	6	NUM
eurjchem-261	73	7	%	%	NOUN
eurjchem-261	73	8	tbab	tbab	NOUN
eurjchem-261	73	9	20/3	20/3	NUM
eurjchem-261	73	10	reflux	reflux	VERB
eurjchem-261	73	11	64.51	64.51	NUM
eurjchem-261	73	12	12	12	NUM
eurjchem-261	73	13	1:2	1:2	NUM
eurjchem-261	73	14	6	6	NUM
eurjchem-261	73	15	%	%	NOUN
eurjchem-261	73	16	tbab	tbab	NOUN
eurjchem-261	73	17	20/3	20/3	NUM
eurjchem-261	73	18	reflux	reflux	VERB
eurjchem-261	73	19	68.61	68.61	NUM
eurjchem-261	73	20	13	13	NUM
eurjchem-261	73	21	1:1	1:1	NUM
eurjchem-261	73	22	6	6	NUM
eurjchem-261	73	23	%	%	NOUN
eurjchem-261	73	24	tbab	tbab	PROPN
eurjchem-261	73	25	20/0	20/0	NUM
eurjchem-261	73	26	reflux	reflux	PROPN
eurjchem-261	73	27	00.00	00.00	NUM
eurjchem-261	73	28	14	14	NUM
eurjchem-261	73	29	1:1	1:1	NUM
eurjchem-261	73	30	6	6	NUM
eurjchem-261	73	31	%	%	NOUN
eurjchem-261	73	32	tbab	tbab	PROPN
eurjchem-261	73	33	20/1	20/1	PROPN
eurjchem-261	73	34	reflux	reflux	VERB
eurjchem-261	73	35	88.11	88.11	NUM
eurjchem-261	73	36	15	15	NUM
eurjchem-261	73	37	1:1	1:1	NUM
eurjchem-261	73	38	6	6	NUM
eurjchem-261	73	39	%	%	NOUN
eurjchem-261	73	40	tbab	tbab	PROPN
eurjchem-261	73	41	20/2	20/2	PROPN
eurjchem-261	73	42	reflux	reflux	NOUN
eurjchem-261	73	43	89.67	89.67	NUM
eurjchem-261	73	44	16	16	NUM
eurjchem-261	73	45	1:1	1:1	NUM
eurjchem-261	73	46	6	6	NUM
eurjchem-261	73	47	%	%	NOUN
eurjchem-261	73	48	tbab	tbab	NOUN
eurjchem-261	73	49	20/5	20/5	NUM
eurjchem-261	73	50	reflux	reflux	NOUN
eurjchem-261	73	51	29.48	29.48	NUM
eurjchem-261	73	52	17	17	NUM
eurjchem-261	73	53	1:1	1:1	NUM
eurjchem-261	73	54	6	6	NUM
eurjchem-261	73	55	%	%	NOUN
eurjchem-261	73	56	tbab	tbab	PROPN
eurjchem-261	73	57	20/2	20/2	NUM
eurjchem-261	73	58	70	70	NUM
eurjchem-261	73	59	60.74	60.74	NUM
eurjchem-261	73	60	18	18	NUM
eurjchem-261	73	61	1:1	1:1	NUM
eurjchem-261	73	62	6	6	NUM
eurjchem-261	73	63	%	%	NOUN
eurjchem-261	73	64	tbab	tbab	PROPN
eurjchem-261	73	65	20/2	20/2	NUM
eurjchem-261	73	66	80	80	NUM
eurjchem-261	73	67	70.16	70.16	NUM
eurjchem-261	73	68	19	19	NUM
eurjchem-261	73	69	1:1	1:1	NUM
eurjchem-261	73	70	6	6	NUM
eurjchem-261	73	71	%	%	NOUN
eurjchem-261	73	72	tbab	tbab	PROPN
eurjchem-261	73	73	20/2	20/2	PROPN
eurjchem-261	73	74	100	100	NUM
eurjchem-261	73	75	86.13	86.13	NUM
eurjchem-261	73	76	a	a	DET
eurjchem-261	73	77	reaction	reaction	NOUN
eurjchem-261	73	78	time	time	NOUN
eurjchem-261	73	79	(	(	PUNCT
eurjchem-261	73	80	11.5	11.5	NUM
eurjchem-261	73	81	h	h	NOUN
eurjchem-261	73	82	)	)	PUNCT
eurjchem-261	73	83	.	.	PUNCT
eurjchem-261	74	1	b	b	X
eurjchem-261	74	2	raw	raw	ADJ
eurjchem-261	74	3	material	material	NOUN
eurjchem-261	74	4	ratio	ratio	NOUN
eurjchem-261	74	5	(	(	PUNCT
eurjchem-261	74	6	sodium	sodium	NOUN
eurjchem-261	74	7	salt	salt	NOUN
eurjchem-261	74	8	of	of	ADP
eurjchem-261	74	9	diethyl	diethyl	NOUN
eurjchem-261	74	10	phosphate	phosphate	NOUN
eurjchem-261	74	11	:	:	PUNCT
eurjchem-261	74	12	benzyl	benzyl	NOUN
eurjchem-261	74	13	chloride	chloride	NOUN
eurjchem-261	74	14	)	)	PUNCT
eurjchem-261	74	15	.	.	PUNCT
eurjchem-261	75	1	c	c	NOUN
eurjchem-261	75	2	the	the	DET
eurjchem-261	75	3	amount	amount	NOUN
eurjchem-261	75	4	of	of	ADP
eurjchem-261	75	5	ptc	ptc	PROPN
eurjchem-261	75	6	is	be	AUX
eurjchem-261	75	7	based	base	VERB
eurjchem-261	75	8	on	on	ADP
eurjchem-261	75	9	sodium	sodium	NOUN
eurjchem-261	75	10	salt	salt	NOUN
eurjchem-261	75	11	of	of	ADP
eurjchem-261	75	12	diethyl	diethyl	NOUN
eurjchem-261	75	13	phosphate	phosphate	NOUN
eurjchem-261	75	14	.	.	PUNCT
eurjchem-261	76	1	d	d	X
eurjchem-261	76	2	refractive	refractive	ADJ
eurjchem-261	76	3	index	index	NOUN
eurjchem-261	76	4	1.4860	1.4860	NUM
eurjchem-261	76	5	(	(	PUNCT
eurjchem-261	76	6	lit	light	VERB
eurjchem-261	76	7	.	.	PUNCT
eurjchem-261	77	1	[	[	X
eurjchem-261	77	2	16	16	NUM
eurjchem-261	77	3	]	]	X
eurjchem-261	77	4	nd20	nd20	PROPN
eurjchem-261	77	5	1.4846	1.4846	NUM
eurjchem-261	77	6	)	)	PUNCT
eurjchem-261	77	7	.	.	PUNCT
eurjchem-261	78	1	e	e	NOUN
eurjchem-261	78	2	isolated	isolate	VERB
eurjchem-261	78	3	yields	yield	NOUN
eurjchem-261	78	4	.	.	PUNCT
eurjchem-261	79	1	the	the	DET
eurjchem-261	79	2	yield	yield	NOUN
eurjchem-261	79	3	and	and	CCONJ
eurjchem-261	79	4	purity	purity	NOUN
eurjchem-261	79	5	consumedly	consumedly	ADV
eurjchem-261	79	6	shrank	shrink	VERB
eurjchem-261	79	7	when	when	SCONJ
eurjchem-261	79	8	the	the	DET
eurjchem-261	79	9	water	water	NOUN
eurjchem-261	79	10	addition	addition	NOUN
eurjchem-261	79	11	was	be	AUX
eurjchem-261	79	12	more	more	ADJ
eurjchem-261	79	13	than	than	ADP
eurjchem-261	79	14	5	5	NUM
eurjchem-261	79	15	ml	ml	NOUN
eurjchem-261	79	16	.	.	PUNCT
eurjchem-261	80	1	further	further	ADJ
eurjchem-261	80	2	addition	addition	NOUN
eurjchem-261	80	3	of	of	ADP
eurjchem-261	80	4	water	water	NOUN
eurjchem-261	80	5	rendered	render	VERB
eurjchem-261	80	6	the	the	DET
eurjchem-261	80	7	conversion	conversion	NOUN
eurjchem-261	80	8	of	of	ADP
eurjchem-261	80	9	the	the	DET
eurjchem-261	80	10	system	system	NOUN
eurjchem-261	80	11	from	from	ADP
eurjchem-261	80	12	s(reagent)‐l(ω)‐	s(reagent)‐l(ω)‐	PROPN
eurjchem-261	80	13	l(org	l(org	PROPN
eurjchem-261	80	14	)	)	PUNCT
eurjchem-261	80	15	to	to	PART
eurjchem-261	80	16	l(ω)‐l(org	l(ω)‐l(org	ADJ
eurjchem-261	80	17	)	)	PUNCT
eurjchem-261	80	18	ptc	ptc	NOUN
eurjchem-261	80	19	,	,	PUNCT
eurjchem-261	80	20	leading	lead	VERB
eurjchem-261	80	21	to	to	ADP
eurjchem-261	80	22	a	a	DET
eurjchem-261	80	23	dramatic	dramatic	ADJ
eurjchem-261	80	24	decrease	decrease	NOUN
eurjchem-261	80	25	in	in	ADP
eurjchem-261	80	26	the	the	DET
eurjchem-261	80	27	effective	effective	ADJ
eurjchem-261	80	28	concentration	concentration	NOUN
eurjchem-261	80	29	of	of	ADP
eurjchem-261	80	30	(	(	PUNCT
eurjchem-261	80	31	eto)2p(o)o‐q+	eto)2p(o)o‐q+	X
eurjchem-261	80	32	in	in	ADP
eurjchem-261	80	33	the	the	DET
eurjchem-261	80	34	organic	organic	ADJ
eurjchem-261	80	35	phase	phase	NOUN
eurjchem-261	80	36	,	,	PUNCT
eurjchem-261	80	37	in	in	ADP
eurjchem-261	80	38	return	return	NOUN
eurjchem-261	80	39	the	the	DET
eurjchem-261	80	40	overall	overall	ADJ
eurjchem-261	80	41	reaction	reaction	NOUN
eurjchem-261	80	42	rate	rate	NOUN
eurjchem-261	80	43	fell	fall	VERB
eurjchem-261	80	44	.	.	PUNCT
eurjchem-261	81	1	thus	thus	ADV
eurjchem-261	81	2	,	,	PUNCT
eurjchem-261	81	3	the	the	DET
eurjchem-261	81	4	2	2	NUM
eurjchem-261	81	5	ml	ml	NOUN
eurjchem-261	81	6	water	water	NOUN
eurjchem-261	81	7	loading	loading	NOUN
eurjchem-261	81	8	helps	help	VERB
eurjchem-261	81	9	to	to	ADP
eurjchem-261	81	10	the	the	DET
eurjchem-261	81	11	reaction	reaction	NOUN
eurjchem-261	81	12	.	.	PUNCT
eurjchem-261	82	1	at	at	ADP
eurjchem-261	82	2	the	the	DET
eurjchem-261	82	3	same	same	ADJ
eurjchem-261	82	4	time	time	NOUN
eurjchem-261	82	5	,	,	PUNCT
eurjchem-261	82	6	it	it	PRON
eurjchem-261	82	7	was	be	AUX
eurjchem-261	82	8	found	find	VERB
eurjchem-261	82	9	when	when	SCONJ
eurjchem-261	82	10	the	the	DET
eurjchem-261	82	11	temperature	temperature	NOUN
eurjchem-261	82	12	was	be	AUX
eurjchem-261	82	13	low	low	ADJ
eurjchem-261	82	14	,	,	PUNCT
eurjchem-261	82	15	the	the	DET
eurjchem-261	82	16	reaction	reaction	NOUN
eurjchem-261	82	17	did	do	AUX
eurjchem-261	82	18	not	not	PART
eurjchem-261	82	19	occur	occur	VERB
eurjchem-261	82	20	.	.	PUNCT
eurjchem-261	83	1	the	the	DET
eurjchem-261	83	2	effect	effect	NOUN
eurjchem-261	83	3	of	of	ADP
eurjchem-261	83	4	temperature	temperature	NOUN
eurjchem-261	83	5	on	on	ADP
eurjchem-261	83	6	the	the	DET
eurjchem-261	83	7	yield	yield	NOUN
eurjchem-261	83	8	of	of	ADP
eurjchem-261	83	9	the	the	DET
eurjchem-261	83	10	product	product	NOUN
eurjchem-261	83	11	was	be	AUX
eurjchem-261	83	12	studied	study	VERB
eurjchem-261	83	13	in	in	ADP
eurjchem-261	83	14	the	the	DET
eurjchem-261	83	15	range	range	NOUN
eurjchem-261	83	16	of	of	ADP
eurjchem-261	83	17	70‐100	70‐100	NUM
eurjchem-261	83	18	°	°	SYM
eurjchem-261	83	19	c	c	NOUN
eurjchem-261	83	20	(	(	PUNCT
eurjchem-261	83	21	entries	entry	NOUN
eurjchem-261	83	22	4	4	NUM
eurjchem-261	83	23	,	,	PUNCT
eurjchem-261	83	24	17‐19	17‐19	NUM
eurjchem-261	83	25	)	)	PUNCT
eurjchem-261	83	26	.	.	PUNCT
eurjchem-261	84	1	the	the	DET
eurjchem-261	84	2	yield	yield	NOUN
eurjchem-261	84	3	was	be	AUX
eurjchem-261	84	4	observed	observe	VERB
eurjchem-261	84	5	to	to	PART
eurjchem-261	84	6	increase	increase	VERB
eurjchem-261	84	7	with	with	ADP
eurjchem-261	84	8	an	an	DET
eurjchem-261	84	9	increase	increase	NOUN
eurjchem-261	84	10	in	in	ADP
eurjchem-261	84	11	the	the	DET
eurjchem-261	84	12	reaction	reaction	NOUN
eurjchem-261	84	13	temperature	temperature	NOUN
eurjchem-261	84	14	up	up	ADP
eurjchem-261	84	15	to	to	PART
eurjchem-261	84	16	reflux	reflux	VERB
eurjchem-261	84	17	for	for	ADP
eurjchem-261	84	18	11.5	11.5	NUM
eurjchem-261	84	19	h.	h.	NOUN
eurjchem-261	84	20	however	however	ADV
eurjchem-261	84	21	,	,	PUNCT
eurjchem-261	84	22	the	the	DET
eurjchem-261	84	23	yield	yield	NOUN
eurjchem-261	84	24	declined	decline	VERB
eurjchem-261	84	25	a	a	DET
eurjchem-261	84	26	little	little	ADJ
eurjchem-261	84	27	when	when	SCONJ
eurjchem-261	84	28	reaction	reaction	NOUN
eurjchem-261	84	29	temperature	temperature	NOUN
eurjchem-261	84	30	was	be	AUX
eurjchem-261	84	31	further	far	ADV
eurjchem-261	84	32	increased	increase	VERB
eurjchem-261	84	33	to	to	ADP
eurjchem-261	84	34	100	100	NUM
eurjchem-261	84	35	°	°	NOUN
eurjchem-261	84	36	c	c	NOUN
eurjchem-261	84	37	,	,	PUNCT
eurjchem-261	84	38	which	which	PRON
eurjchem-261	84	39	may	may	AUX
eurjchem-261	84	40	be	be	AUX
eurjchem-261	84	41	resulted	result	VERB
eurjchem-261	84	42	in	in	ADP
eurjchem-261	84	43	an	an	DET
eurjchem-261	84	44	evaporation	evaporation	NOUN
eurjchem-261	84	45	of	of	ADP
eurjchem-261	84	46	the	the	DET
eurjchem-261	84	47	ω‐phase	ω‐phase	NUM
eurjchem-261	84	48	water	water	NOUN
eurjchem-261	84	49	at	at	ADP
eurjchem-261	84	50	this	this	DET
eurjchem-261	84	51	temperature	temperature	NOUN
eurjchem-261	84	52	.	.	PUNCT
eurjchem-261	85	1	as	as	ADP
eurjchem-261	85	2	a	a	DET
eurjchem-261	85	3	result	result	NOUN
eurjchem-261	85	4	,	,	PUNCT
eurjchem-261	85	5	the	the	DET
eurjchem-261	85	6	reflux	reflux	NOUN
eurjchem-261	85	7	temperature	temperature	NOUN
eurjchem-261	85	8	was	be	AUX
eurjchem-261	85	9	chosen	choose	VERB
eurjchem-261	85	10	to	to	PART
eurjchem-261	85	11	be	be	AUX
eurjchem-261	85	12	the	the	DET
eurjchem-261	85	13	optimized	optimize	VERB
eurjchem-261	85	14	temperature	temperature	NOUN
eurjchem-261	85	15	.	.	PUNCT
eurjchem-261	86	1	in	in	ADP
eurjchem-261	86	2	conclusion	conclusion	NOUN
eurjchem-261	86	3	,	,	PUNCT
eurjchem-261	86	4	at	at	ADP
eurjchem-261	86	5	the	the	DET
eurjchem-261	86	6	optimized	optimize	VERB
eurjchem-261	86	7	reaction	reaction	NOUN
eurjchem-261	86	8	conditions	condition	NOUN
eurjchem-261	86	9	,	,	PUNCT
eurjchem-261	86	10	the	the	DET
eurjchem-261	86	11	catalytic	catalytic	ADJ
eurjchem-261	86	12	efficiency	efficiency	NOUN
eurjchem-261	86	13	was	be	AUX
eurjchem-261	86	14	tbab	tbab	PROPN
eurjchem-261	86	15	>	>	X
eurjchem-261	86	16	ctab	ctab	PROPN
eurjchem-261	86	17	>	>	X
eurjchem-261	86	18	teba	teba	PROPN
eurjchem-261	86	19	>	>	X
eurjchem-261	86	20	peg‐400	peg‐400	PROPN
eurjchem-261	86	21	.	.	PUNCT
eurjchem-261	87	1	the	the	DET
eurjchem-261	87	2	amounts	amount	NOUN
eurjchem-261	87	3	of	of	ADP
eurjchem-261	87	4	catalyst	catalyst	NOUN
eurjchem-261	87	5	was	be	AUX
eurjchem-261	87	6	6	6	NUM
eurjchem-261	87	7	mol%	mol%	PROPN
eurjchem-261	87	8	tbab	tbab	PROPN
eurjchem-261	87	9	.	.	PUNCT
eurjchem-261	88	1	the	the	DET
eurjchem-261	88	2	raw	raw	ADJ
eurjchem-261	88	3	material	material	NOUN
eurjchem-261	88	4	ratio	ratio	NOUN
eurjchem-261	88	5	of	of	ADP
eurjchem-261	88	6	sodium	sodium	NOUN
eurjchem-261	88	7	salt	salt	NOUN
eurjchem-261	88	8	of	of	ADP
eurjchem-261	88	9	diethyl	diethyl	NOUN
eurjchem-261	88	10	phosphate	phosphate	NOUN
eurjchem-261	88	11	to	to	PART
eurjchem-261	88	12	benzyl	benzyl	VERB
eurjchem-261	88	13	chloride	chloride	NOUN
eurjchem-261	88	14	was	be	AUX
eurjchem-261	88	15	1:1	1:1	NUM
eurjchem-261	88	16	.	.	PUNCT
eurjchem-261	89	1	the	the	DET
eurjchem-261	89	2	quantity	quantity	NOUN
eurjchem-261	89	3	of	of	ADP
eurjchem-261	89	4	water	water	NOUN
eurjchem-261	89	5	added	add	VERB
eurjchem-261	89	6	was	be	AUX
eurjchem-261	89	7	2	2	NUM
eurjchem-261	89	8	ml	ml	NOUN
eurjchem-261	89	9	per	per	ADP
eurjchem-261	89	10	0.05	0.05	NUM
eurjchem-261	89	11	mol	mol	ADP
eurjchem-261	89	12	sodium	sodium	NOUN
eurjchem-261	89	13	salt	salt	NOUN
eurjchem-261	89	14	of	of	ADP
eurjchem-261	89	15	diethyl	diethyl	NOUN
eurjchem-261	89	16	phosphate	phosphate	NOUN
eurjchem-261	89	17	.	.	PUNCT
eurjchem-261	90	1	the	the	DET
eurjchem-261	90	2	reaction	reaction	NOUN
eurjchem-261	90	3	temperature	temperature	NOUN
eurjchem-261	90	4	is	be	AUX
eurjchem-261	90	5	the	the	DET
eurjchem-261	90	6	reflux	reflux	NOUN
eurjchem-261	90	7	temperature	temperature	NOUN
eurjchem-261	90	8	of	of	ADP
eurjchem-261	90	9	the	the	DET
eurjchem-261	90	10	mixed	mixed	ADJ
eurjchem-261	90	11	solvents	solvent	NOUN
eurjchem-261	90	12	.	.	PUNCT
eurjchem-261	91	1	acknowledgements	acknowledgement	NOUN
eurjchem-261	91	2	the	the	DET
eurjchem-261	91	3	authors	author	NOUN
eurjchem-261	91	4	wish	wish	VERB
eurjchem-261	91	5	to	to	PART
eurjchem-261	91	6	acknowledge	acknowledge	VERB
eurjchem-261	91	7	their	their	PRON
eurjchem-261	91	8	gratitude	gratitude	NOUN
eurjchem-261	91	9	to	to	ADP
eurjchem-261	91	10	daqing	daqe	VERB
eurjchem-261	91	11	new	new	ADJ
eurjchem-261	91	12	century	century	NOUN
eurjchem-261	91	13	fine	fine	PROPN
eurjchem-261	91	14	chemicals	chemicals	PROPN
eurjchem-261	91	15	co.	co.	PROPN
eurjchem-261	91	16	,	,	PUNCT
eurjchem-261	91	17	ltd	ltd	PROPN
eurjchem-261	91	18	.	.	PROPN
eurjchem-261	91	19	for	for	ADP
eurjchem-261	91	20	the	the	DET
eurjchem-261	91	21	by‐product	by‐product	NOUN
eurjchem-261	91	22	of	of	ADP
eurjchem-261	91	23	fluorescent	fluorescent	ADJ
eurjchem-261	91	24	brightener	brightener	NOUN
eurjchem-261	91	25	support	support	NOUN
eurjchem-261	91	26	.	.	PUNCT
eurjchem-261	92	1	references	reference	NOUN
eurjchem-261	92	2	[	[	X
eurjchem-261	92	3	1	1	NUM
eurjchem-261	92	4	]	]	PUNCT
eurjchem-261	92	5	.	.	PUNCT
eurjchem-261	93	1	macquarrie	macquarrie	PROPN
eurjchem-261	93	2	,	,	PUNCT
eurjchem-261	93	3	d.	d.	PROPN
eurjchem-261	93	4	j.	j.	PROPN
eurjchem-261	93	5	;	;	PUNCT
eurjchem-261	93	6	nazih	nazih	PROPN
eurjchem-261	93	7	,	,	PUNCT
eurjchem-261	93	8	r.	r.	PROPN
eurjchem-261	93	9	;	;	PUNCT
eurjchem-261	93	10	sebti	sebti	PROPN
eurjchem-261	93	11	,	,	PUNCT
eurjchem-261	93	12	s.	s.	PROPN
eurjchem-261	93	13	green	green	PROPN
eurjchem-261	93	14	chem	chem	PROPN
eurjchem-261	93	15	.	.	PUNCT
eurjchem-261	94	1	2002	2002	NUM
eurjchem-261	94	2	,	,	PUNCT
eurjchem-261	94	3	4	4	NUM
eurjchem-261	94	4	,	,	PUNCT
eurjchem-261	94	5	56‐59	56‐59	NUM
eurjchem-261	94	6	.	.	PUNCT
eurjchem-261	95	1	[	[	X
eurjchem-261	95	2	2	2	NUM
eurjchem-261	95	3	]	]	PUNCT
eurjchem-261	95	4	.	.	PUNCT
eurjchem-261	96	1	fraile	fraile	PROPN
eurjchem-261	96	2	,	,	PUNCT
eurjchem-261	96	3	j.	j.	PROPN
eurjchem-261	96	4	m.	m.	PROPN
eurjchem-261	96	5	;	;	PUNCT
eurjchem-261	96	6	garcía	garcía	PROPN
eurjchem-261	96	7	,	,	PUNCT
eurjchem-261	96	8	j.	j.	PROPN
eurjchem-261	96	9	i.	i.	PROPN
eurjchem-261	96	10	;	;	PUNCT
eurjchem-261	96	11	mayoral	mayoral	ADJ
eurjchem-261	96	12	,	,	PUNCT
eurjchem-261	96	13	j.	j.	PROPN
eurjchem-261	96	14	a.	a.	PROPN
eurjchem-261	96	15	;	;	PUNCT
eurjchem-261	96	16	sebti	sebti	PROPN
eurjchem-261	96	17	,	,	PUNCT
eurjchem-261	96	18	s.	s.	PROPN
eurjchem-261	96	19	;	;	PUNCT
eurjchem-261	96	20	tahir	tahir	PROPN
eurjchem-261	96	21	,	,	PUNCT
eurjchem-261	96	22	r.	r.	PROPN
eurjchem-261	96	23	green	green	PROPN
eurjchem-261	96	24	chem	chem	PROPN
eurjchem-261	96	25	.	.	PUNCT
eurjchem-261	97	1	2001	2001	NUM
eurjchem-261	97	2	,	,	PUNCT
eurjchem-261	97	3	3	3	NUM
eurjchem-261	97	4	,	,	PUNCT
eurjchem-261	97	5	271‐274	271‐274	NUM
eurjchem-261	97	6	.	.	PUNCT
eurjchem-261	98	1	[	[	X
eurjchem-261	98	2	3	3	NUM
eurjchem-261	98	3	]	]	PUNCT
eurjchem-261	98	4	.	.	PUNCT
eurjchem-261	99	1	silverberg	silverberg	PROPN
eurjchem-261	99	2	,	,	PUNCT
eurjchem-261	99	3	l.	l.	PROPN
eurjchem-261	99	4	j.	j.	PROPN
eurjchem-261	99	5	;	;	PUNCT
eurjchem-261	99	6	dillon	dillon	PROPN
eurjchem-261	99	7	,	,	PUNCT
eurjchem-261	99	8	j.	j.	PROPN
eurjchem-261	99	9	l.	l.	PROPN
eurjchem-261	99	10	;	;	PUNCT
eurjchem-261	99	11	vemishetti	vemishetti	PROPN
eurjchem-261	99	12	,	,	PUNCT
eurjchem-261	99	13	p.	p.	NOUN
eurjchem-261	99	14	tetrahedron	tetrahedron	PROPN
eurjchem-261	99	15	lett	lett	PROPN
eurjchem-261	99	16	.	.	PUNCT
eurjchem-261	99	17	1996	1996	NUM
eurjchem-261	99	18	,	,	PUNCT
eurjchem-261	99	19	37	37	NUM
eurjchem-261	99	20	,	,	PUNCT
eurjchem-261	99	21	771‐774	771‐774	NUM
eurjchem-261	99	22	.	.	PUNCT
eurjchem-261	100	1	[	[	X
eurjchem-261	100	2	4	4	NUM
eurjchem-261	100	3	]	]	PUNCT
eurjchem-261	100	4	.	.	PUNCT
eurjchem-261	101	1	jones	jones	PROPN
eurjchem-261	101	2	,	,	PUNCT
eurjchem-261	101	3	s.	s.	PROPN
eurjchem-261	101	4	;	;	PUNCT
eurjchem-261	101	5	smanmoo	smanmoo	NOUN
eurjchem-261	101	6	,	,	PUNCT
eurjchem-261	101	7	c.	c.	PROPN
eurjchem-261	101	8	tetrahedron	tetrahedron	PROPN
eurjchem-261	101	9	lett	lett	PROPN
eurjchem-261	101	10	.	.	PUNCT
eurjchem-261	102	1	2004	2004	NUM
eurjchem-261	102	2	,	,	PUNCT
eurjchem-261	102	3	45	45	NUM
eurjchem-261	102	4	,	,	PUNCT
eurjchem-261	102	5	1585‐1588	1585‐1588	NUM
eurjchem-261	102	6	.	.	PUNCT
eurjchem-261	103	1	[	[	X
eurjchem-261	103	2	5	5	NUM
eurjchem-261	103	3	]	]	PUNCT
eurjchem-261	103	4	.	.	PUNCT
eurjchem-261	103	5	bache	bache	PROPN
eurjchem-261	103	6	,	,	PUNCT
eurjchem-261	103	7	c.	c.	PROPN
eurjchem-261	103	8	a.	a.	PROPN
eurjchem-261	103	9	;	;	PUNCT
eurjchem-261	103	10	lisk	lisk	PROPN
eurjchem-261	103	11	,	,	PUNCT
eurjchem-261	103	12	d.	d.	PROPN
eurjchem-261	103	13	j.	j.	PROPN
eurjchem-261	103	14	anal	anal	PROPN
eurjchem-261	103	15	.	.	PUNCT
eurjchem-261	103	16	chem	chem	PROPN
eurjchem-261	103	17	.	.	PUNCT
eurjchem-261	104	1	1965	1965	NUM
eurjchem-261	104	2	,	,	PUNCT
eurjchem-261	104	3	37	37	NUM
eurjchem-261	104	4	,	,	PUNCT
eurjchem-261	104	5	1477‐1480	1477‐1480	NUM
eurjchem-261	104	6	.	.	PUNCT
eurjchem-261	105	1	[	[	X
eurjchem-261	105	2	6	6	NUM
eurjchem-261	105	3	]	]	PUNCT
eurjchem-261	105	4	.	.	PUNCT
eurjchem-261	105	5	brown	brown	PROPN
eurjchem-261	105	6	,	,	PUNCT
eurjchem-261	105	7	d.	d.	PROPN
eurjchem-261	105	8	m.	m.	PROPN
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eurjchem-261	105	10	in	in	ADP
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eurjchem-261	105	12	chemistry	chemistry	NOUN
eurjchem-261	105	13	,	,	PUNCT
eurjchem-261	105	14	interscience	interscience	NOUN
eurjchem-261	105	15	publishers	publisher	NOUN
eurjchem-261	105	16	,	,	PUNCT
eurjchem-261	105	17	inc	inc	PROPN
eurjchem-261	105	18	.	.	PROPN
eurjchem-261	105	19	,	,	PUNCT
eurjchem-261	105	20	new	new	PROPN
eurjchem-261	105	21	york	york	PROPN
eurjchem-261	105	22	,	,	PUNCT
eurjchem-261	105	23	1963	1963	NUM
eurjchem-261	105	24	,	,	PUNCT
eurjchem-261	105	25	vol	vol	NOUN
eurjchem-261	105	26	.	.	PROPN
eurjchem-261	105	27	3	3	NUM
eurjchem-261	105	28	,	,	PUNCT
eurjchem-261	105	29	89‐90	89‐90	NUM
eurjchem-261	105	30	.	.	PUNCT
eurjchem-261	106	1	[	[	X
eurjchem-261	106	2	7	7	NUM
eurjchem-261	106	3	]	]	PUNCT
eurjchem-261	106	4	.	.	PUNCT
eurjchem-261	107	1	slotin	slotin	PROPN
eurjchem-261	107	2	,	,	PUNCT
eurjchem-261	107	3	l.	l.	PROPN
eurjchem-261	107	4	a.	a.	NOUN
eurjchem-261	107	5	synthesis	synthesis	PROPN
eurjchem-261	107	6	1977	1977	NUM
eurjchem-261	107	7	,	,	PUNCT
eurjchem-261	107	8	737‐752	737‐752	NUM
eurjchem-261	107	9	.	.	PUNCT
eurjchem-261	108	1	[	[	X
eurjchem-261	108	2	8	8	NUM
eurjchem-261	108	3	]	]	PUNCT
eurjchem-261	108	4	.	.	PUNCT
eurjchem-261	109	1	cherbuliez	cherbuliez	PROPN
eurjchem-261	109	2	,	,	PUNCT
eurjchem-261	109	3	e.	e.	PROPN
eurjchem-261	109	4	;	;	PUNCT
eurjchem-261	109	5	kosolapoff	kosolapoff	PROPN
eurjchem-261	109	6	,	,	PUNCT
eurjchem-261	109	7	g.	g.	PROPN
eurjchem-261	109	8	m.	m.	PROPN
eurjchem-261	109	9	l.	l.	PROPN
eurjchem-261	109	10	;	;	PUNCT
eurjchem-261	109	11	eds	ed	NOUN
eurjchem-261	109	12	,	,	PUNCT
eurjchem-261	109	13	m.	m.	NOUN
eurjchem-261	109	14	in	in	ADP
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eurjchem-261	109	17	chemistry	chemistry	NOUN
eurjchem-261	109	18	,	,	PUNCT
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eurjchem-261	109	20	,	,	PUNCT
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eurjchem-261	109	23	,	,	PUNCT
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eurjchem-261	109	25	,	,	PUNCT
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eurjchem-261	109	29	,	,	PUNCT
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eurjchem-261	109	32	.	.	PUNCT
eurjchem-261	110	1	[	[	X
eurjchem-261	110	2	9	9	NUM
eurjchem-261	110	3	]	]	PUNCT
eurjchem-261	110	4	.	.	PUNCT
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eurjchem-261	111	2	,	,	PUNCT
eurjchem-261	111	3	j.	j.	PROPN
eurjchem-261	111	4	i.	i.	PROPN
eurjchem-261	111	5	g.	g.	PROPN
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eurjchem-261	111	8	in	in	ADP
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eurjchem-261	111	11	,	,	PUNCT
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eurjchem-261	111	14	,	,	PUNCT
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eurjchem-261	111	16	,	,	PUNCT
eurjchem-261	111	17	london	london	PROPN
eurjchem-261	111	18	,	,	PUNCT
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eurjchem-261	111	20	.	.	PUNCT
eurjchem-261	112	1	[	[	X
eurjchem-261	112	2	10	10	NUM
eurjchem-261	112	3	]	]	PUNCT
eurjchem-261	112	4	.	.	PUNCT
eurjchem-261	113	1	mclaughlin	mclaughlin	PROPN
eurjchem-261	113	2	,	,	PUNCT
eurjchem-261	113	3	m.	m.	NOUN
eurjchem-261	113	4	org	org	PROPN
eurjchem-261	113	5	.	.	PUNCT
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eurjchem-261	114	2	.	.	PUNCT
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eurjchem-261	115	2	,	,	PUNCT
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eurjchem-261	115	4	,	,	PUNCT
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eurjchem-261	115	6	.	.	PUNCT
eurjchem-261	116	1	[	[	X
eurjchem-261	116	2	11	11	NUM
eurjchem-261	116	3	]	]	PUNCT
eurjchem-261	116	4	.	.	PUNCT
eurjchem-261	117	1	kofink	kofink	PROPN
eurjchem-261	117	2	,	,	PUNCT
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eurjchem-261	117	5	;	;	PUNCT
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eurjchem-261	117	10	.	.	PUNCT
eurjchem-261	118	1	lett	lett	PROPN
eurjchem-261	118	2	.	.	PUNCT
eurjchem-261	119	1	2006	2006	NUM
eurjchem-261	119	2	,	,	PUNCT
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eurjchem-261	119	4	,	,	PUNCT
eurjchem-261	119	5	4121‐4124	4121‐4124	NUM
eurjchem-261	119	6	.	.	PUNCT
eurjchem-261	120	1	[	[	X
eurjchem-261	120	2	12	12	NUM
eurjchem-261	120	3	]	]	PUNCT
eurjchem-261	120	4	.	.	PUNCT
eurjchem-261	121	1	kenner	kenner	PROPN
eurjchem-261	121	2	,	,	PUNCT
eurjchem-261	121	3	g.	g.	PROPN
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eurjchem-261	121	5	;	;	PUNCT
eurjchem-261	121	6	mather	mather	PROPN
eurjchem-261	121	7	,	,	PUNCT
eurjchem-261	121	8	j.	j.	PROPN
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eurjchem-261	122	2	.	.	PUNCT
eurjchem-261	123	1	1956	1956	NUM
eurjchem-261	123	2	,	,	PUNCT
eurjchem-261	123	3	3524‐3531	3524‐3531	NUM
eurjchem-261	123	4	.	.	PUNCT
eurjchem-261	124	1	[	[	X
eurjchem-261	124	2	13	13	NUM
eurjchem-261	124	3	]	]	PUNCT
eurjchem-261	124	4	.	.	PUNCT
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eurjchem-261	125	2	,	,	PUNCT
eurjchem-261	125	3	y.	y.	PROPN
eurjchem-261	125	4	;	;	PUNCT
eurjchem-261	125	5	arakawa	arakawa	PROPN
eurjchem-261	125	6	,	,	PUNCT
eurjchem-261	125	7	y.	y.	PROPN
eurjchem-261	125	8	chem	chem	PROPN
eurjchem-261	125	9	.	.	PUNCT
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eurjchem-261	126	2	.	.	PUNCT
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eurjchem-261	127	2	.	.	PUNCT
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eurjchem-261	128	2	,	,	PUNCT
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eurjchem-261	128	4	,	,	PUNCT
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eurjchem-261	128	6	.	.	PUNCT
eurjchem-261	129	1	[	[	X
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eurjchem-261	129	3	]	]	PUNCT
eurjchem-261	129	4	.	.	PUNCT
eurjchem-261	130	1	givens	givens	PROPN
eurjchem-261	130	2	,	,	PUNCT
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eurjchem-261	130	5	;	;	PUNCT
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eurjchem-261	130	7	,	,	PUNCT
eurjchem-261	130	8	b.	b.	PROPN
eurjchem-261	130	9	;	;	PUNCT
eurjchem-261	130	10	athey	athey	PROPN
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eurjchem-261	130	14	;	;	PUNCT
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eurjchem-261	130	21	.	.	PUNCT
eurjchem-261	131	1	chem	chem	PROPN
eurjchem-261	131	2	.	.	PUNCT
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eurjchem-261	132	2	.	.	PUNCT
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eurjchem-261	133	2	,	,	PUNCT
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eurjchem-261	133	4	,	,	PUNCT
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eurjchem-261	133	6	.	.	PUNCT
eurjchem-261	134	1	[	[	X
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eurjchem-261	134	3	]	]	PUNCT
eurjchem-261	134	4	.	.	PUNCT
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eurjchem-261	135	2	,	,	PUNCT
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eurjchem-261	135	4	;	;	PUNCT
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eurjchem-261	136	3	]	]	PUNCT
eurjchem-261	136	4	.	.	PUNCT
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eurjchem-261	136	6	,	,	PUNCT
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eurjchem-261	136	14	.	.	PUNCT
eurjchem-261	137	1	[	[	X
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eurjchem-261	137	3	]	]	PUNCT
eurjchem-261	137	4	.	.	PUNCT
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eurjchem-261	138	2	,	,	PUNCT
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eurjchem-261	138	5	;	;	PUNCT
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eurjchem-261	138	7	,	,	PUNCT
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eurjchem-261	139	2	.	.	PUNCT
eurjchem-261	140	1	a	a	DET
eurjchem-261	140	2	:	:	PUNCT
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eurjchem-261	140	4	.	.	PUNCT
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eurjchem-261	141	2	,	,	PUNCT
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eurjchem-261	141	4	,	,	PUNCT
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eurjchem-261	141	6	.	.	PUNCT
eurjchem-261	142	1	[	[	X
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eurjchem-261	142	3	]	]	PUNCT
eurjchem-261	142	4	.	.	PUNCT
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eurjchem-261	143	2	,	,	PUNCT
eurjchem-261	143	3	h.	h.	PROPN
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eurjchem-261	143	5	;	;	PUNCT
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eurjchem-261	143	7	,	,	PUNCT
eurjchem-261	143	8	p.	p.	PROPN
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eurjchem-261	143	10	appl	appl	PROPN
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eurjchem-261	144	2	.	.	PUNCT
eurjchem-261	145	1	a	a	DET
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eurjchem-261	145	3	,	,	PUNCT
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eurjchem-261	145	5	,	,	PUNCT
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eurjchem-261	145	7	.	.	PUNCT
eurjchem-261	146	1	[	[	X
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eurjchem-261	146	3	]	]	PUNCT
eurjchem-261	146	4	.	.	PUNCT
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eurjchem-261	147	2	,	,	PUNCT
eurjchem-261	147	3	h.	h.	PROPN
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eurjchem-261	147	5	;	;	PUNCT
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eurjchem-261	147	7	,	,	PUNCT
eurjchem-261	147	8	h.‐c	h.‐c	PROPN
eurjchem-261	147	9	.	.	PUNCT
eurjchem-261	148	1	appl	appl	PROPN
eurjchem-261	148	2	.	.	PUNCT
eurjchem-261	149	1	catal	catal	PROPN
eurjchem-261	149	2	.	.	PUNCT
eurjchem-261	150	1	a	a	DET
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eurjchem-261	150	3	,	,	PUNCT
eurjchem-261	150	4	258	258	NUM
eurjchem-261	150	5	,	,	PUNCT
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eurjchem-261	150	7	.	.	PUNCT
eurjchem-261	151	1	[	[	X
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eurjchem-261	151	3	]	]	PUNCT
eurjchem-261	151	4	.	.	PUNCT
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eurjchem-261	152	2	,	,	PUNCT
eurjchem-261	152	3	g.	g.	PROPN
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eurjchem-261	152	5	;	;	PUNCT
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eurjchem-261	152	7	,	,	PUNCT
eurjchem-261	152	8	j.	j.	PROPN
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eurjchem-261	152	10	j.	j.	PROPN
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eurjchem-261	153	1	catal	catal	PROPN
eurjchem-261	153	2	.	.	PUNCT
eurjchem-261	153	3	a.	a.	NOUN
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eurjchem-261	153	5	.	.	PUNCT
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eurjchem-261	154	2	,	,	PUNCT
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eurjchem-261	154	4	,	,	PUNCT
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eurjchem-261	155	1	[	[	X
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eurjchem-261	155	3	]	]	PUNCT
eurjchem-261	155	4	.	.	PUNCT
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eurjchem-261	156	2	,	,	PUNCT
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eurjchem-261	156	5	;	;	PUNCT
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eurjchem-261	156	7	,	,	PUNCT
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eurjchem-261	156	13	.	.	PUNCT
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eurjchem-261	157	2	,	,	PUNCT
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eurjchem-261	157	4	,	,	PUNCT
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eurjchem-261	157	6	.	.	PUNCT
eurjchem-261	158	1	[	[	X
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eurjchem-261	158	4	.	.	PUNCT
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eurjchem-261	159	2	,	,	PUNCT
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eurjchem-261	159	5	;	;	PUNCT
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eurjchem-261	160	5	.	.	PUNCT
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eurjchem-261	161	2	,	,	PUNCT
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eurjchem-261	161	4	,	,	PUNCT
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eurjchem-261	161	6	.	.	PUNCT
eurjchem-261	162	1	[	[	X
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eurjchem-261	162	4	.	.	PUNCT
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eurjchem-261	163	2	,	,	PUNCT
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eurjchem-261	163	5	;	;	PUNCT
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eurjchem-261	163	7	,	,	PUNCT
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