id	sid	tid	token	lemma	pos
eurjchem-267	1	1	untitled	untitle	VERB
eurjchem-267	1	2	european	european	PROPN
eurjchem-267	1	3	journal	journal	PROPN
eurjchem-267	1	4	of	of	ADP
eurjchem-267	1	5	chemistry	chemistry	NOUN
eurjchem-267	1	6	2	2	NUM
eurjchem-267	1	7	(	(	PUNCT
eurjchem-267	1	8	3	3	NUM
eurjchem-267	1	9	)	)	PUNCT
eurjchem-267	1	10	(	(	PUNCT
eurjchem-267	1	11	2011	2011	NUM
eurjchem-267	1	12	)	)	PUNCT
eurjchem-267	1	13	404‐409	404‐409	NUM
eurjchem-267	1	14	european	european	ADJ
eurjchem-267	1	15	journal	journal	PROPN
eurjchem-267	1	16	of	of	ADP
eurjchem-267	1	17	chemistry	chemistry	NOUN
eurjchem-267	1	18	issn	issn	PROPN
eurjchem-267	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-267	1	20	(	(	PUNCT
eurjchem-267	1	21	print	print	NOUN
eurjchem-267	1	22	)	)	PUNCT
eurjchem-267	1	23	/	/	SYM
eurjchem-267	1	24	issn	issn	PROPN
eurjchem-267	1	25	2153‐2257	2153‐2257	NUM
eurjchem-267	1	26	(	(	PUNCT
eurjchem-267	1	27	online	online	ADJ
eurjchem-267	1	28	)	)	PUNCT
eurjchem-267	1	29			NOUN
eurjchem-267	1	30	2011	2011	NUM
eurjchem-267	1	31	eurjchem	eurjchem	PROPN
eurjchem-267	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-267	1	33	/	/	SYM
eurjchem-267	1	34	eurjchem.2.3.404‐409.267	eurjchem.2.3.404‐409.267	NOUN
eurjchem-267	1	35	european	european	ADJ
eurjchem-267	1	36	journal	journal	PROPN
eurjchem-267	1	37	of	of	ADP
eurjchem-267	1	38	chemistry	chemistry	PROPN
eurjchem-267	1	39	journal	journal	PROPN
eurjchem-267	1	40	homepage	homepage	NOUN
eurjchem-267	1	41	:	:	PUNCT
eurjchem-267	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-267	1	43	synthesis	synthesis	NOUN
eurjchem-267	1	44	of	of	ADP
eurjchem-267	1	45	novel	novel	ADJ
eurjchem-267	1	46	quinazolinone	quinazolinone	NOUN
eurjchem-267	1	47	and	and	CCONJ
eurjchem-267	1	48	fused	fuse	VERB
eurjchem-267	1	49	quinazolinones	quinazolinone	NOUN
eurjchem-267	1	50	mahmoud	mahmoud	PROPN
eurjchem-267	1	51	refaee	refaee	PROPN
eurjchem-267	1	52	mahmoud	mahmoud	PROPN
eurjchem-267	1	53	,	,	PUNCT
eurjchem-267	1	54	manal	manal	PROPN
eurjchem-267	1	55	mohamed	mohamed	PROPN
eurjchem-267	1	56	el‐shahawi	el‐shahawi	PROPN
eurjchem-267	1	57	and	and	CCONJ
eurjchem-267	1	58	fatma	fatma	PROPN
eurjchem-267	1	59	saber	saber	PROPN
eurjchem-267	1	60	mohamed	mohamed	PROPN
eurjchem-267	1	61	abu	abu	PROPN
eurjchem-267	1	62	el‐azm	el‐azm	PROPN
eurjchem-267	1	63	*	*	PROPN
eurjchem-267	1	64	chemistry	chemistry	NOUN
eurjchem-267	1	65	department	department	NOUN
eurjchem-267	1	66	,	,	PUNCT
eurjchem-267	1	67	faculty	faculty	NOUN
eurjchem-267	1	68	of	of	ADP
eurjchem-267	1	69	science	science	NOUN
eurjchem-267	1	70	,	,	PUNCT
eurjchem-267	1	71	ain	ain	PROPN
eurjchem-267	1	72	shams	shams	PROPN
eurjchem-267	1	73	university	university	PROPN
eurjchem-267	1	74	,	,	PUNCT
eurjchem-267	1	75	abbassia	abbassia	NOUN
eurjchem-267	1	76	11566	11566	NUM
eurjchem-267	1	77	,	,	PUNCT
eurjchem-267	1	78	cairo	cairo	PROPN
eurjchem-267	1	79	,	,	PUNCT
eurjchem-267	1	80	egypt	egypt	PROPN
eurjchem-267	1	81	*	*	PUNCT
eurjchem-267	1	82	corresponding	correspond	VERB
eurjchem-267	1	83	author	author	NOUN
eurjchem-267	1	84	at	at	ADP
eurjchem-267	1	85	:	:	PUNCT
eurjchem-267	1	86	chemistry	chemistry	NOUN
eurjchem-267	1	87	department	department	NOUN
eurjchem-267	1	88	,	,	PUNCT
eurjchem-267	1	89	faculty	faculty	NOUN
eurjchem-267	1	90	of	of	ADP
eurjchem-267	1	91	science	science	NOUN
eurjchem-267	1	92	,	,	PUNCT
eurjchem-267	1	93	ain	ain	PROPN
eurjchem-267	1	94	shams	shams	PROPN
eurjchem-267	1	95	university	university	PROPN
eurjchem-267	1	96	,	,	PUNCT
eurjchem-267	1	97	abbassia	abbassia	NOUN
eurjchem-267	1	98	11566	11566	NUM
eurjchem-267	1	99	,	,	PUNCT
eurjchem-267	1	100	cairo	cairo	PROPN
eurjchem-267	1	101	,	,	PUNCT
eurjchem-267	1	102	egypt	egypt	PROPN
eurjchem-267	1	103	.	.	PUNCT
eurjchem-267	2	1	tel	tel	PROPN
eurjchem-267	2	2	.	.	PUNCT
eurjchem-267	2	3	:	:	PUNCT
eurjchem-267	3	1	+010.9756276	+010.9756276	NOUN
eurjchem-267	3	2	;	;	PUNCT
eurjchem-267	3	3	fax	fax	NOUN
eurjchem-267	3	4	:	:	PUNCT
eurjchem-267	3	5	+202.831836	+202.831836	PROPN
eurjchem-267	3	6	.	.	PUNCT
eurjchem-267	3	7	e‐mail	e‐mail	PUNCT
eurjchem-267	4	1	address	address	NOUN
eurjchem-267	4	2	:	:	PUNCT
eurjchem-267	4	3	ftmsaber@yahoo.com	ftmsaber@yahoo.com	X
eurjchem-267	4	4	(	(	PUNCT
eurjchem-267	4	5	f.s.m	f.s.m	NOUN
eurjchem-267	4	6	.	.	PUNCT
eurjchem-267	5	1	abu	abu	PROPN
eurjchem-267	5	2	el‐azm	el‐azm	PROPN
eurjchem-267	5	3	)	)	PUNCT
eurjchem-267	5	4	.	.	PUNCT
eurjchem-267	6	1	article	article	NOUN
eurjchem-267	6	2	information	information	PROPN
eurjchem-267	6	3	abstract	abstract	ADV
eurjchem-267	6	4	received	receive	VERB
eurjchem-267	6	5	:	:	PUNCT
eurjchem-267	6	6	28	28	NUM
eurjchem-267	6	7	august	august	PROPN
eurjchem-267	6	8	2010	2010	NUM
eurjchem-267	6	9	received	receive	VERB
eurjchem-267	6	10	in	in	ADP
eurjchem-267	6	11	revised	revise	VERB
eurjchem-267	6	12	form	form	NOUN
eurjchem-267	6	13	:	:	PUNCT
eurjchem-267	6	14	13	13	NUM
eurjchem-267	6	15	october	october	NOUN
eurjchem-267	6	16	2010	2010	NUM
eurjchem-267	6	17	accepted	accept	VERB
eurjchem-267	6	18	:	:	PUNCT
eurjchem-267	6	19	04	04	NUM
eurjchem-267	6	20	january	january	PROPN
eurjchem-267	6	21	2011	2011	NUM
eurjchem-267	6	22	online	online	ADV
eurjchem-267	6	23	:	:	PUNCT
eurjchem-267	6	24	30	30	NUM
eurjchem-267	6	25	september	september	PROPN
eurjchem-267	6	26	2011	2011	NUM
eurjchem-267	6	27	keywords	keyword	VERB
eurjchem-267	6	28	a	a	DET
eurjchem-267	6	29	number	number	NOUN
eurjchem-267	6	30	of	of	ADP
eurjchem-267	6	31	novel	novel	ADJ
eurjchem-267	6	32	quinazolinone	quinazolinone	NOUN
eurjchem-267	6	33	derivatives	derivative	NOUN
eurjchem-267	6	34	have	have	AUX
eurjchem-267	6	35	been	be	AUX
eurjchem-267	6	36	synthesized	synthesize	VERB
eurjchem-267	6	37	using	use	VERB
eurjchem-267	6	38	the	the	DET
eurjchem-267	6	39	readily	readily	ADV
eurjchem-267	6	40	obtainable	obtainable	ADJ
eurjchem-267	6	41	2‐[(1z,3e)‐1‐benzamido‐4‐phenyl‐1,3‐butadien‐1‐yl]‐3,1‐benzoxazin‐4(h)one	2‐[(1z,3e)‐1‐benzamido‐4‐phenyl‐1,3‐butadien‐1‐yl]‐3,1‐benzoxazin‐4(h)one	NUM
eurjchem-267	6	42	(	(	PUNCT
eurjchem-267	6	43	1	1	NUM
eurjchem-267	6	44	)	)	PUNCT
eurjchem-267	6	45	via	via	ADP
eurjchem-267	6	46	the	the	DET
eurjchem-267	6	47	reaction	reaction	NOUN
eurjchem-267	6	48	with	with	ADP
eurjchem-267	6	49	different	different	ADJ
eurjchem-267	6	50	nitrogen	nitrogen	NOUN
eurjchem-267	6	51	nucleophiles	nucleophile	NOUN
eurjchem-267	6	52	such	such	ADJ
eurjchem-267	6	53	as	as	ADP
eurjchem-267	6	54	azines	azine	NOUN
eurjchem-267	6	55	,	,	PUNCT
eurjchem-267	6	56	schiff	schiff	PROPN
eurjchem-267	6	57	’s	’s	PART
eurjchem-267	6	58	base	base	NOUN
eurjchem-267	6	59	,	,	PUNCT
eurjchem-267	6	60	primary	primary	ADJ
eurjchem-267	6	61	aromatic	aromatic	ADJ
eurjchem-267	6	62	amines	amine	NOUN
eurjchem-267	6	63	,	,	PUNCT
eurjchem-267	6	64	diamines	diamine	NOUN
eurjchem-267	6	65	,	,	PUNCT
eurjchem-267	6	66	hydrazine	hydrazine	NOUN
eurjchem-267	6	67	hydrate	hydrate	NOUN
eurjchem-267	6	68	and	and	CCONJ
eurjchem-267	6	69	hydroxylamine	hydroxylamine	NOUN
eurjchem-267	6	70	.	.	PUNCT
eurjchem-267	7	1	benzoxazinone	benzoxazinone	NOUN
eurjchem-267	7	2	azine	azine	PROPN
eurjchem-267	7	3	fused	fuse	VERB
eurjchem-267	7	4	quinazolinones	quinazolinone	NOUN
eurjchem-267	7	5	nitrogen	nitrogen	NOUN
eurjchem-267	7	6	nucleophiles	nucleophile	NOUN
eurjchem-267	7	7	triazinoquinazolinone	triazinoquinazolinone	NOUN
eurjchem-267	7	8	oxadiazinoquinazolinone	oxadiazinoquinazolinone	NOUN
eurjchem-267	7	9	1	1	NUM
eurjchem-267	7	10	.	.	PUNCT
eurjchem-267	8	1	introduction	introduction	NOUN
eurjchem-267	8	2	benzoxazinones	benzoxazinone	NOUN
eurjchem-267	8	3	(	(	PUNCT
eurjchem-267	8	4	bas	bas	X
eurjchem-267	8	5	)	)	PUNCT
eurjchem-267	8	6	are	be	AUX
eurjchem-267	8	7	natural	natural	ADJ
eurjchem-267	8	8	products	product	NOUN
eurjchem-267	8	9	that	that	PRON
eurjchem-267	8	10	are	be	AUX
eurjchem-267	8	11	present	present	ADJ
eurjchem-267	8	12	in	in	ADP
eurjchem-267	8	13	gramineae	gramineae	PROPN
eurjchem-267	9	1	[	[	X
eurjchem-267	9	2	1	1	NUM
eurjchem-267	9	3	]	]	PUNCT
eurjchem-267	9	4	and	and	CCONJ
eurjchem-267	9	5	represent	represent	VERB
eurjchem-267	9	6	part	part	NOUN
eurjchem-267	9	7	of	of	ADP
eurjchem-267	9	8	the	the	DET
eurjchem-267	9	9	plant	plant	NOUN
eurjchem-267	9	10	defense	defense	NOUN
eurjchem-267	9	11	system	system	NOUN
eurjchem-267	9	12	against	against	ADP
eurjchem-267	9	13	pests	pest	NOUN
eurjchem-267	9	14	,	,	PUNCT
eurjchem-267	9	15	including	include	VERB
eurjchem-267	9	16	insects	insect	NOUN
eurjchem-267	9	17	,	,	PUNCT
eurjchem-267	9	18	bacteria	bacteria	NOUN
eurjchem-267	9	19	and	and	CCONJ
eurjchem-267	9	20	fungi	fungus	NOUN
eurjchem-267	10	1	[	[	X
eurjchem-267	10	2	2,3	2,3	NUM
eurjchem-267	10	3	]	]	PUNCT
eurjchem-267	10	4	.	.	PUNCT
eurjchem-267	11	1	several	several	ADJ
eurjchem-267	11	2	studies	study	NOUN
eurjchem-267	11	3	on	on	ADP
eurjchem-267	11	4	the	the	DET
eurjchem-267	11	5	acute	acute	ADJ
eurjchem-267	11	6	toxic	toxic	ADJ
eurjchem-267	11	7	effects	effect	NOUN
eurjchem-267	11	8	of	of	ADP
eurjchem-267	11	9	bas	bas	PROPN
eurjchem-267	11	10	in	in	ADP
eurjchem-267	11	11	insects	insect	NOUN
eurjchem-267	11	12	and	and	CCONJ
eurjchem-267	11	13	bacteria	bacteria	NOUN
eurjchem-267	11	14	have	have	AUX
eurjchem-267	11	15	been	be	AUX
eurjchem-267	11	16	published	publish	VERB
eurjchem-267	11	17	[	[	PUNCT
eurjchem-267	11	18	4‐8	4‐8	NOUN
eurjchem-267	11	19	]	]	PUNCT
eurjchem-267	11	20	.	.	PUNCT
eurjchem-267	12	1	quinazolinone	quinazolinone	PROPN
eurjchem-267	12	2	alkaloids	alkaloid	NOUN
eurjchem-267	12	3	possess	possess	VERB
eurjchem-267	12	4	a	a	DET
eurjchem-267	12	5	diverse	diverse	ADJ
eurjchem-267	12	6	range	range	NOUN
eurjchem-267	12	7	of	of	ADP
eurjchem-267	12	8	biological	biological	ADJ
eurjchem-267	12	9	activities	activity	NOUN
eurjchem-267	12	10	including	include	VERB
eurjchem-267	12	11	cytotoxicity	cytotoxicity	NOUN
eurjchem-267	12	12	[	[	X
eurjchem-267	12	13	9	9	NUM
eurjchem-267	12	14	]	]	PUNCT
eurjchem-267	12	15	,	,	PUNCT
eurjchem-267	12	16	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-267	13	1	[	[	X
eurjchem-267	13	2	10	10	NUM
eurjchem-267	13	3	]	]	PUNCT
eurjchem-267	13	4	,	,	PUNCT
eurjchem-267	13	5	anticancer	anticancer	NOUN
eurjchem-267	13	6	,	,	PUNCT
eurjchem-267	13	7	antimicrobial	antimicrobial	ADJ
eurjchem-267	13	8	,	,	PUNCT
eurjchem-267	13	9	anticonvulsant	anticonvulsant	NOUN
eurjchem-267	13	10	[	[	X
eurjchem-267	13	11	11‐15	11‐15	NUM
eurjchem-267	13	12	]	]	PUNCT
eurjchem-267	13	13	and	and	CCONJ
eurjchem-267	13	14	cardiovascular	cardiovascular	ADJ
eurjchem-267	13	15	activity	activity	NOUN
eurjchem-267	14	1	[	[	X
eurjchem-267	14	2	16,17	16,17	NUM
eurjchem-267	14	3	]	]	PUNCT
eurjchem-267	14	4	.	.	PUNCT
eurjchem-267	15	1	these	these	DET
eurjchem-267	15	2	compounds	compound	NOUN
eurjchem-267	15	3	also	also	ADV
eurjchem-267	15	4	act	act	VERB
eurjchem-267	15	5	as	as	ADP
eurjchem-267	15	6	cardiotonic	cardiotonic	ADJ
eurjchem-267	15	7	,	,	PUNCT
eurjchem-267	15	8	antihistaminic	antihistaminic	NOUN
eurjchem-267	15	9	,	,	PUNCT
eurjchem-267	15	10	antifungal	antifungal	PROPN
eurjchem-267	15	11	,	,	PUNCT
eurjchem-267	15	12	antiviral	antiviral	ADJ
eurjchem-267	15	13	,	,	PUNCT
eurjchem-267	15	14	antimycobacterial	antimycobacterial	ADJ
eurjchem-267	15	15	and	and	CCONJ
eurjchem-267	15	16	antimalarial	antimalarial	ADJ
eurjchem-267	15	17	agents	agent	NOUN
eurjchem-267	15	18	[	[	X
eurjchem-267	15	19	18‐24	18‐24	X
eurjchem-267	15	20	]	]	PUNCT
eurjchem-267	15	21	and	and	CCONJ
eurjchem-267	15	22	they	they	PRON
eurjchem-267	15	23	have	have	AUX
eurjchem-267	15	24	demonstrated	demonstrate	VERB
eurjchem-267	15	25	psychotropic	psychotropic	ADJ
eurjchem-267	15	26	,	,	PUNCT
eurjchem-267	15	27	hypnotic	hypnotic	ADJ
eurjchem-267	15	28	and	and	CCONJ
eurjchem-267	15	29	a	a	DET
eurjchem-267	15	30	range	range	NOUN
eurjchem-267	15	31	of	of	ADP
eurjchem-267	15	32	other	other	ADJ
eurjchem-267	15	33	central	central	ADJ
eurjchem-267	15	34	nervous	nervous	ADJ
eurjchem-267	15	35	system	system	NOUN
eurjchem-267	15	36	(	(	PUNCT
eurjchem-267	15	37	cns	cns	NOUN
eurjchem-267	15	38	)	)	PUNCT
eurjchem-267	15	39	effects	effect	NOUN
eurjchem-267	16	1	[	[	X
eurjchem-267	16	2	25‐27	25‐27	NOUN
eurjchem-267	16	3	]	]	PUNCT
eurjchem-267	16	4	.	.	PUNCT
eurjchem-267	17	1	in	in	ADP
eurjchem-267	17	2	view	view	NOUN
eurjchem-267	17	3	of	of	ADP
eurjchem-267	17	4	their	their	PRON
eurjchem-267	17	5	natural	natural	ADJ
eurjchem-267	17	6	occurrence	occurrence	NOUN
eurjchem-267	17	7	,	,	PUNCT
eurjchem-267	17	8	biological	biological	ADJ
eurjchem-267	17	9	activities	activity	NOUN
eurjchem-267	17	10	and	and	CCONJ
eurjchem-267	17	11	utility	utility	NOUN
eurjchem-267	17	12	as	as	ADP
eurjchem-267	17	13	synthetic	synthetic	ADJ
eurjchem-267	17	14	intermediates	intermediate	NOUN
eurjchem-267	17	15	[	[	X
eurjchem-267	17	16	28‐33	28‐33	NUM
eurjchem-267	17	17	]	]	PUNCT
eurjchem-267	17	18	,	,	PUNCT
eurjchem-267	17	19	we	we	PRON
eurjchem-267	17	20	report	report	VERB
eurjchem-267	17	21	here	here	ADV
eurjchem-267	17	22	the	the	DET
eurjchem-267	17	23	synthesis	synthesis	NOUN
eurjchem-267	17	24	of	of	ADP
eurjchem-267	17	25	novel	novel	ADJ
eurjchem-267	17	26	benzoxazinone	benzoxazinone	NOUN
eurjchem-267	17	27	and	and	CCONJ
eurjchem-267	17	28	quinazolinone	quinazolinone	NOUN
eurjchem-267	17	29	derivatives	derivative	NOUN
eurjchem-267	17	30	starting	start	VERB
eurjchem-267	17	31	from	from	ADP
eurjchem-267	17	32	the	the	DET
eurjchem-267	17	33	readily	readily	ADV
eurjchem-267	17	34	obtainable	obtainable	ADJ
eurjchem-267	17	35	2‐[(1z,3e)‐1‐benzamido‐4‐phenyl‐1,3‐	2‐[(1z,3e)‐1‐benzamido‐4‐phenyl‐1,3‐	NUM
eurjchem-267	17	36	butadien‐1‐yl]‐3,1‐benzoxazin‐4(h)one	butadien‐1‐yl]‐3,1‐benzoxazin‐4(h)one	NUM
eurjchem-267	17	37	(	(	PUNCT
eurjchem-267	17	38	1	1	X
eurjchem-267	17	39	)	)	PUNCT
eurjchem-267	17	40	which	which	PRON
eurjchem-267	17	41	prepared	prepare	VERB
eurjchem-267	17	42	via	via	ADP
eurjchem-267	17	43	the	the	DET
eurjchem-267	17	44	reaction	reaction	NOUN
eurjchem-267	17	45	of	of	ADP
eurjchem-267	17	46	oxazolone	oxazolone	NOUN
eurjchem-267	17	47	derivative	derivative	NOUN
eurjchem-267	17	48	with	with	ADP
eurjchem-267	17	49	anthranilic	anthranilic	ADJ
eurjchem-267	17	50	acid	acid	NOUN
eurjchem-267	17	51	in	in	ADP
eurjchem-267	17	52	boiling	boil	VERB
eurjchem-267	17	53	acetic	acetic	ADJ
eurjchem-267	17	54	acid	acid	NOUN
eurjchem-267	17	55	according	accord	VERB
eurjchem-267	17	56	to	to	ADP
eurjchem-267	17	57	the	the	DET
eurjchem-267	17	58	published	publish	VERB
eurjchem-267	17	59	procedure	procedure	NOUN
eurjchem-267	17	60	[	[	X
eurjchem-267	17	61	34	34	NUM
eurjchem-267	17	62	]	]	PUNCT
eurjchem-267	17	63	.	.	PUNCT
eurjchem-267	18	1	2	2	X
eurjchem-267	18	2	.	.	X
eurjchem-267	18	3	experimental	experimental	ADJ
eurjchem-267	18	4	all	all	DET
eurjchem-267	18	5	melting	melt	VERB
eurjchem-267	18	6	points	point	NOUN
eurjchem-267	18	7	were	be	AUX
eurjchem-267	18	8	taken	take	VERB
eurjchem-267	18	9	on	on	ADP
eurjchem-267	18	10	griffin	griffin	NOUN
eurjchem-267	18	11	and	and	CCONJ
eurjchem-267	18	12	geory	geory	NOUN
eurjchem-267	18	13	melting	melting	NOUN
eurjchem-267	18	14	point	point	NOUN
eurjchem-267	18	15	apparatus	apparatus	NOUN
eurjchem-267	18	16	and	and	CCONJ
eurjchem-267	18	17	are	be	AUX
eurjchem-267	18	18	uncorrected	uncorrecte	VERB
eurjchem-267	18	19	.	.	PUNCT
eurjchem-267	19	1	ir	ir	PROPN
eurjchem-267	19	2	spectra	spectra	PROPN
eurjchem-267	19	3	were	be	AUX
eurjchem-267	19	4	recorded	record	VERB
eurjchem-267	19	5	on	on	ADP
eurjchem-267	19	6	pye	pye	PROPN
eurjchem-267	19	7	unicam	unicam	PROPN
eurjchem-267	19	8	sp1200	sp1200	PROPN
eurjchem-267	19	9	spectrophotometer	spectrophotometer	NOUN
eurjchem-267	19	10	using	use	VERB
eurjchem-267	19	11	kbr	kbr	PROPN
eurjchem-267	19	12	wafer	wafer	NOUN
eurjchem-267	19	13	technique	technique	NOUN
eurjchem-267	19	14	.	.	PUNCT
eurjchem-267	20	1	1h	1h	NUM
eurjchem-267	20	2	nmr	nmr	PROPN
eurjchem-267	20	3	spectra	spectra	NOUN
eurjchem-267	20	4	were	be	AUX
eurjchem-267	20	5	determined	determine	VERB
eurjchem-267	20	6	on	on	ADP
eurjchem-267	20	7	a	a	DET
eurjchem-267	20	8	varian	varian	PROPN
eurjchem-267	20	9	gemini	gemini	PROPN
eurjchem-267	20	10	200	200	NUM
eurjchem-267	20	11	mhz	mhz	NOUN
eurjchem-267	20	12	using	use	VERB
eurjchem-267	20	13	tms	tms	PROPN
eurjchem-267	20	14	as	as	ADP
eurjchem-267	20	15	internal	internal	ADJ
eurjchem-267	20	16	standard	standard	NOUN
eurjchem-267	20	17	(	(	PUNCT
eurjchem-267	20	18	chemical	chemical	ADJ
eurjchem-267	20	19	shifts	shift	NOUN
eurjchem-267	20	20	in	in	ADP
eurjchem-267	20	21	δ‐scale	δ‐scale	NOUN
eurjchem-267	20	22	)	)	PUNCT
eurjchem-267	20	23	.	.	PUNCT
eurjchem-267	21	1	ei‐ms	ei‐ms	PROPN
eurjchem-267	21	2	were	be	AUX
eurjchem-267	21	3	measured	measure	VERB
eurjchem-267	21	4	on	on	ADP
eurjchem-267	21	5	a	a	DET
eurjchem-267	21	6	shimadzu‐gc‐ms	shimadzu‐gc‐ms	NOUN
eurjchem-267	21	7	operating	operate	VERB
eurjchem-267	21	8	at	at	ADP
eurjchem-267	21	9	70	70	NUM
eurjchem-267	21	10	ev	ev	NOUN
eurjchem-267	21	11	.	.	PROPN
eurjchem-267	21	12	13c	13c	NOUN
eurjchem-267	21	13	nmr	nmr	NOUN
eurjchem-267	21	14	spectra	spectra	NOUN
eurjchem-267	21	15	were	be	AUX
eurjchem-267	21	16	measured	measure	VERB
eurjchem-267	21	17	on	on	ADP
eurjchem-267	21	18	jool	jool	NOUN
eurjchem-267	21	19	75	75	NUM
eurjchem-267	21	20	mhz	mhz	NOUN
eurjchem-267	21	21	.	.	PUNCT
eurjchem-267	22	1	elemental	elemental	ADJ
eurjchem-267	22	2	analyses	analysis	NOUN
eurjchem-267	22	3	were	be	AUX
eurjchem-267	22	4	carried	carry	VERB
eurjchem-267	22	5	out	out	ADP
eurjchem-267	22	6	at	at	ADP
eurjchem-267	22	7	the	the	DET
eurjchem-267	22	8	microanalytical	microanalytical	ADJ
eurjchem-267	22	9	unit	unit	NOUN
eurjchem-267	22	10	,	,	PUNCT
eurjchem-267	22	11	faculty	faculty	NOUN
eurjchem-267	22	12	of	of	ADP
eurjchem-267	22	13	science	science	NOUN
eurjchem-267	22	14	,	,	PUNCT
eurjchem-267	22	15	ain	ain	PROPN
eurjchem-267	22	16	shams	sham	NOUN
eurjchem-267	22	17	university	university	NOUN
eurjchem-267	22	18	by	by	ADP
eurjchem-267	22	19	using	use	VERB
eurjchem-267	22	20	perkin‐elmer	perkin‐elmer	PROPN
eurjchem-267	22	21	2400	2400	NUM
eurjchem-267	22	22	chn	chn	PROPN
eurjchem-267	22	23	elemental	elemental	ADJ
eurjchem-267	22	24	analyzer	analyzer	NOUN
eurjchem-267	22	25	and	and	CCONJ
eurjchem-267	22	26	satisfactory	satisfactory	ADJ
eurjchem-267	22	27	analytical	analytical	ADJ
eurjchem-267	22	28	data	datum	NOUN
eurjchem-267	22	29	(	(	PUNCT
eurjchem-267	22	30	±	±	NOUN
eurjchem-267	22	31	0.4	0.4	NUM
eurjchem-267	22	32	)	)	PUNCT
eurjchem-267	22	33	were	be	AUX
eurjchem-267	22	34	obtained	obtain	VERB
eurjchem-267	22	35	for	for	ADP
eurjchem-267	22	36	all	all	DET
eurjchem-267	22	37	compounds	compound	NOUN
eurjchem-267	22	38	.	.	PUNCT
eurjchem-267	23	1	the	the	DET
eurjchem-267	23	2	homogeneity	homogeneity	NOUN
eurjchem-267	23	3	of	of	ADP
eurjchem-267	23	4	the	the	DET
eurjchem-267	23	5	synthesized	synthesize	VERB
eurjchem-267	23	6	compounds	compound	NOUN
eurjchem-267	23	7	was	be	AUX
eurjchem-267	23	8	controlled	control	VERB
eurjchem-267	23	9	by	by	ADP
eurjchem-267	23	10	tlc	tlc	NOUN
eurjchem-267	24	1	[	[	X
eurjchem-267	24	2	using	use	VERB
eurjchem-267	24	3	tlc	tlc	NOUN
eurjchem-267	24	4	aluminum	aluminum	NOUN
eurjchem-267	24	5	sheets	sheet	NOUN
eurjchem-267	24	6	silica	silica	NOUN
eurjchem-267	24	7	gel	gel	NOUN
eurjchem-267	24	8	f254	f254	PROPN
eurjchem-267	24	9	(	(	PUNCT
eurjchem-267	24	10	merck	merck	PROPN
eurjchem-267	24	11	)	)	PUNCT
eurjchem-267	24	12	]	]	PUNCT
eurjchem-267	24	13	.	.	PUNCT
eurjchem-267	25	1	2.1	2.1	NUM
eurjchem-267	25	2	.	.	PUNCT
eurjchem-267	26	1	2‐[(1z,3e)‐1‐benzamido‐4‐phenyl‐1,3‐butadien‐1‐yl]‐	2‐[(1z,3e)‐1‐benzamido‐4‐phenyl‐1,3‐butadien‐1‐yl]‐	NUM
eurjchem-267	26	2	3,1‐benzoxazin‐4(h)‐one	3,1‐benzoxazin‐4(h)‐one	NUM
eurjchem-267	26	3	(	(	PUNCT
eurjchem-267	26	4	1	1	NUM
eurjchem-267	26	5	)	)	PUNCT
eurjchem-267	26	6	a	a	DET
eurjchem-267	26	7	mixture	mixture	NOUN
eurjchem-267	26	8	of	of	ADP
eurjchem-267	26	9	4‐cinnamylidene‐2‐phenyl‐∆2‐oxazol‐5‐one	4‐cinnamylidene‐2‐phenyl‐∆2‐oxazol‐5‐one	NUM
eurjchem-267	26	10	(	(	PUNCT
eurjchem-267	26	11	2.73	2.73	NUM
eurjchem-267	26	12	g	g	NOUN
eurjchem-267	26	13	,	,	PUNCT
eurjchem-267	26	14	0.01	0.01	NUM
eurjchem-267	26	15	mol	mol	NOUN
eurjchem-267	26	16	)	)	PUNCT
eurjchem-267	26	17	and	and	CCONJ
eurjchem-267	26	18	anthranilic	anthranilic	ADJ
eurjchem-267	26	19	acid	acid	NOUN
eurjchem-267	26	20	(	(	PUNCT
eurjchem-267	26	21	1.37	1.37	NUM
eurjchem-267	26	22	g	g	NOUN
eurjchem-267	26	23	,	,	PUNCT
eurjchem-267	26	24	0.01	0.01	NUM
eurjchem-267	26	25	mol	mol	NOUN
eurjchem-267	26	26	)	)	PUNCT
eurjchem-267	26	27	in	in	ADP
eurjchem-267	26	28	acetic	acetic	ADJ
eurjchem-267	26	29	acid	acid	NOUN
eurjchem-267	26	30	(	(	PUNCT
eurjchem-267	26	31	20	20	NUM
eurjchem-267	26	32	ml	ml	NOUN
eurjchem-267	26	33	)	)	PUNCT
eurjchem-267	26	34	and	and	CCONJ
eurjchem-267	26	35	freshly	freshly	ADV
eurjchem-267	26	36	distilled	distil	VERB
eurjchem-267	26	37	acetic	acetic	ADJ
eurjchem-267	26	38	anhydride	anhydride	NOUN
eurjchem-267	26	39	(	(	PUNCT
eurjchem-267	26	40	10	10	NUM
eurjchem-267	26	41	ml	ml	NOUN
eurjchem-267	26	42	)	)	PUNCT
eurjchem-267	26	43	was	be	AUX
eurjchem-267	26	44	refluxed	refluxe	VERB
eurjchem-267	26	45	for	for	ADP
eurjchem-267	26	46	10	10	NUM
eurjchem-267	26	47	hrs	hrs	NOUN
eurjchem-267	26	48	until	until	ADP
eurjchem-267	26	49	no	no	DET
eurjchem-267	26	50	more	more	ADJ
eurjchem-267	26	51	substrate	substrate	NOUN
eurjchem-267	26	52	(	(	PUNCT
eurjchem-267	26	53	tlc	tlc	NOUN
eurjchem-267	26	54	)	)	PUNCT
eurjchem-267	26	55	.	.	PUNCT
eurjchem-267	27	1	the	the	DET
eurjchem-267	27	2	reaction	reaction	NOUN
eurjchem-267	27	3	mixture	mixture	NOUN
eurjchem-267	27	4	was	be	AUX
eurjchem-267	27	5	poured	pour	VERB
eurjchem-267	27	6	on	on	ADP
eurjchem-267	27	7	water	water	NOUN
eurjchem-267	27	8	(	(	PUNCT
eurjchem-267	27	9	100	100	NUM
eurjchem-267	27	10	ml	ml	NOUN
eurjchem-267	27	11	)	)	PUNCT
eurjchem-267	27	12	and	and	CCONJ
eurjchem-267	27	13	stirred	stir	VERB
eurjchem-267	27	14	for	for	ADP
eurjchem-267	27	15	20	20	NUM
eurjchem-267	27	16	min	min	NOUN
eurjchem-267	27	17	.	.	PUNCT
eurjchem-267	28	1	the	the	DET
eurjchem-267	28	2	yellow	yellow	ADJ
eurjchem-267	28	3	solid	solid	ADJ
eurjchem-267	28	4	separated	separate	VERB
eurjchem-267	28	5	was	be	AUX
eurjchem-267	28	6	collected	collect	VERB
eurjchem-267	28	7	by	by	ADP
eurjchem-267	28	8	filtration	filtration	NOUN
eurjchem-267	28	9	,	,	PUNCT
eurjchem-267	28	10	washed	wash	VERB
eurjchem-267	28	11	with	with	ADP
eurjchem-267	28	12	water	water	NOUN
eurjchem-267	28	13	several	several	ADJ
eurjchem-267	28	14	times	time	NOUN
eurjchem-267	28	15	,	,	PUNCT
eurjchem-267	28	16	then	then	ADV
eurjchem-267	28	17	with	with	ADP
eurjchem-267	28	18	sodium	sodium	NOUN
eurjchem-267	28	19	bicarbonate	bicarbonate	NOUN
eurjchem-267	28	20	solution	solution	NOUN
eurjchem-267	28	21	(	(	PUNCT
eurjchem-267	28	22	10	10	NUM
eurjchem-267	28	23	%	%	NOUN
eurjchem-267	28	24	,	,	PUNCT
eurjchem-267	28	25	40	40	NUM
eurjchem-267	28	26	ml	ml	NOUN
eurjchem-267	28	27	)	)	PUNCT
eurjchem-267	28	28	.	.	PUNCT
eurjchem-267	29	1	the	the	DET
eurjchem-267	29	2	solid	solid	ADJ
eurjchem-267	29	3	was	be	AUX
eurjchem-267	29	4	filtered	filter	VERB
eurjchem-267	29	5	off	off	ADP
eurjchem-267	29	6	,	,	PUNCT
eurjchem-267	29	7	washed	wash	VERB
eurjchem-267	29	8	with	with	ADP
eurjchem-267	29	9	water	water	NOUN
eurjchem-267	29	10	,	,	PUNCT
eurjchem-267	29	11	dried	dry	VERB
eurjchem-267	29	12	and	and	CCONJ
eurjchem-267	29	13	then	then	ADV
eurjchem-267	29	14	recrystallized	recrystallize	VERB
eurjchem-267	29	15	from	from	ADP
eurjchem-267	29	16	ethanol	ethanol	NOUN
eurjchem-267	29	17	to	to	PART
eurjchem-267	29	18	give	give	VERB
eurjchem-267	29	19	1	1	NUM
eurjchem-267	29	20	as	as	ADP
eurjchem-267	29	21	lemon	lemon	NOUN
eurjchem-267	29	22	yellow	yellow	ADJ
eurjchem-267	29	23	crystals	crystal	NOUN
eurjchem-267	29	24	.	.	PUNCT
eurjchem-267	30	1	yield	yield	NOUN
eurjchem-267	30	2	:	:	PUNCT
eurjchem-267	30	3	64	64	NUM
eurjchem-267	30	4	%	%	NOUN
eurjchem-267	30	5	.	.	PUNCT
eurjchem-267	31	1	m.p	m.p	PROPN
eurjchem-267	31	2	.	.	PROPN
eurjchem-267	31	3	:	:	PUNCT
eurjchem-267	31	4	84‐86	84‐86	NOUN
eurjchem-267	31	5	oc	oc	PROPN
eurjchem-267	31	6	.	.	PROPN
eurjchem-267	31	7	ft‐ir	ft‐ir	NOUN
eurjchem-267	31	8	(	(	PUNCT
eurjchem-267	31	9	kbr	kbr	PROPN
eurjchem-267	31	10	,	,	PUNCT
eurjchem-267	31	11	cm‐1	cm‐1	PROPN
eurjchem-267	31	12	):	):	PUNCT
eurjchem-267	31	13	3292	3292	NUM
eurjchem-267	31	14	ν(nh	ν(nh	NOUN
eurjchem-267	31	15	)	)	PUNCT
eurjchem-267	31	16	,	,	PUNCT
eurjchem-267	31	17	1771	1771	NUM
eurjchem-267	31	18	ν(c	ν(c	NOUN
eurjchem-267	31	19	=	=	SYM
eurjchem-267	31	20	oδ‐lactone	oδ‐lactone	NOUN
eurjchem-267	31	21	)	)	PUNCT
eurjchem-267	31	22	,	,	PUNCT
eurjchem-267	31	23	1678	1678	NUM
eurjchem-267	31	24	ν(c	ν(c	NOUN
eurjchem-267	31	25	=	=	SYM
eurjchem-267	31	26	oamide	oamide	ADV
eurjchem-267	31	27	)	)	PUNCT
eurjchem-267	31	28	,	,	PUNCT
eurjchem-267	31	29	1642	1642	NUM
eurjchem-267	31	30	ν(c	ν(c	NOUN
eurjchem-267	31	31	=	=	SYM
eurjchem-267	31	32	n	n	NUM
eurjchem-267	31	33	)	)	PUNCT
eurjchem-267	31	34	.	.	PUNCT
eurjchem-267	32	1	1h	1h	NUM
eurjchem-267	32	2	nmr	nmr	NOUN
eurjchem-267	32	3	(	(	PUNCT
eurjchem-267	32	4	200	200	NUM
eurjchem-267	32	5	mhz	mhz	NOUN
eurjchem-267	32	6	,	,	PUNCT
eurjchem-267	32	7	cdcl3	cdcl3	NOUN
eurjchem-267	32	8	):	):	PUNCT
eurjchem-267	32	9	8.90	8.90	NUM
eurjchem-267	32	10	(	(	PUNCT
eurjchem-267	32	11	s	s	PROPN
eurjchem-267	32	12	,	,	PUNCT
eurjchem-267	32	13	1h	1h	NUM
eurjchem-267	32	14	,	,	PUNCT
eurjchem-267	32	15	nh	nh	PROPN
eurjchem-267	32	16	,	,	PUNCT
eurjchem-267	32	17	exchangeable	exchangeable	ADJ
eurjchem-267	32	18	with	with	ADP
eurjchem-267	32	19	d2o	d2o	NOUN
eurjchem-267	32	20	)	)	PUNCT
eurjchem-267	32	21	,	,	PUNCT
eurjchem-267	32	22	8.08‐7.40	8.08‐7.40	NUM
eurjchem-267	32	23	(	(	PUNCT
eurjchem-267	32	24	m	m	PROPN
eurjchem-267	32	25	,	,	PUNCT
eurjchem-267	32	26	14harom	14harom	NUM
eurjchem-267	32	27	.	.	PUNCT
eurjchem-267	32	28	)	)	PUNCT
eurjchem-267	32	29	,	,	PUNCT
eurjchem-267	32	30	7.10‐	7.10‐	NUM
eurjchem-267	32	31	5.60	5.60	NUM
eurjchem-267	32	32	(	(	PUNCT
eurjchem-267	32	33	m	m	PROPN
eurjchem-267	32	34	,	,	PUNCT
eurjchem-267	32	35	3h	3h	NUM
eurjchem-267	32	36	)	)	PUNCT
eurjchem-267	32	37	.	.	PUNCT
eurjchem-267	33	1	13c	13c	NOUN
eurjchem-267	33	2	nmr	nmr	NOUN
eurjchem-267	33	3	(	(	PUNCT
eurjchem-267	33	4	200	200	NUM
eurjchem-267	33	5	mhz	mhz	NOUN
eurjchem-267	33	6	,	,	PUNCT
eurjchem-267	33	7	cdcl3	cdcl3	NOUN
eurjchem-267	33	8	):	):	PUNCT
eurjchem-267	33	9	167.1	167.1	NUM
eurjchem-267	33	10	(	(	PUNCT
eurjchem-267	33	11	coamide	coamide	ADJ
eurjchem-267	33	12	)	)	PUNCT
eurjchem-267	33	13	,	,	PUNCT
eurjchem-267	33	14	160.1	160.1	NUM
eurjchem-267	33	15	(	(	PUNCT
eurjchem-267	33	16	c4	c4	NOUN
eurjchem-267	33	17	)	)	PUNCT
eurjchem-267	33	18	,	,	PUNCT
eurjchem-267	33	19	158.2	158.2	NUM
eurjchem-267	33	20	(	(	PUNCT
eurjchem-267	33	21	c2	c2	PROPN
eurjchem-267	33	22	)	)	PUNCT
eurjchem-267	33	23	,	,	PUNCT
eurjchem-267	33	24	133.7	133.7	NUM
eurjchem-267	33	25	(	(	PUNCT
eurjchem-267	33	26	c4	c4	NOUN
eurjchem-267	33	27	’	'	PUNCT
eurjchem-267	33	28	)	)	PUNCT
eurjchem-267	33	29	,	,	PUNCT
eurjchem-267	33	30	134.1	134.1	NUM
eurjchem-267	33	31	(	(	PUNCT
eurjchem-267	33	32	c5	c5	PROPN
eurjchem-267	33	33	)	)	PUNCT
eurjchem-267	33	34	,	,	PUNCT
eurjchem-267	33	35	130.1	130.1	NUM
eurjchem-267	33	36	(	(	PUNCT
eurjchem-267	33	37	c7	c7	PROPN
eurjchem-267	33	38	)	)	PUNCT
eurjchem-267	33	39	,	,	PUNCT
eurjchem-267	33	40	128.6	128.6	NUM
eurjchem-267	33	41	(	(	PUNCT
eurjchem-267	33	42	c6	c6	PROPN
eurjchem-267	33	43	)	)	PUNCT
eurjchem-267	33	44	,	,	PUNCT
eurjchem-267	33	45	127.2	127.2	NUM
eurjchem-267	33	46	(	(	PUNCT
eurjchem-267	33	47	c8	c8	PROPN
eurjchem-267	33	48	)	)	PUNCT
eurjchem-267	33	49	,	,	PUNCT
eurjchem-267	33	50	126.3	126.3	NUM
eurjchem-267	33	51	(	(	PUNCT
eurjchem-267	33	52	c3	c3	PROPN
eurjchem-267	33	53	’	'	PUNCT
eurjchem-267	33	54	)	)	PUNCT
eurjchem-267	33	55	,	,	PUNCT
eurjchem-267	33	56	120.3	120.3	NUM
eurjchem-267	33	57	(	(	PUNCT
eurjchem-267	33	58	c1	c1	PROPN
eurjchem-267	33	59	’	'	PUNCT
eurjchem-267	33	60	)	)	PUNCT
eurjchem-267	33	61	,	,	PUNCT
eurjchem-267	33	62	109.3	109.3	NUM
eurjchem-267	33	63	(	(	PUNCT
eurjchem-267	33	64	c2	c2	PROPN
eurjchem-267	33	65	’	'	PUNCT
eurjchem-267	33	66	)	)	PUNCT
eurjchem-267	33	67	,	,	PUNCT
eurjchem-267	33	68	133.2	133.2	NUM
eurjchem-267	33	69	,	,	PUNCT
eurjchem-267	33	70	128.1	128.1	NUM
eurjchem-267	33	71	,	,	PUNCT
eurjchem-267	33	72	126.6	126.6	NUM
eurjchem-267	33	73	,	,	PUNCT
eurjchem-267	33	74	130.2	130.2	NUM
eurjchem-267	33	75	(	(	PUNCT
eurjchem-267	33	76	phenyl	phenyl	NOUN
eurjchem-267	33	77	of	of	ADP
eurjchem-267	33	78	benzamido	benzamido	NOUN
eurjchem-267	33	79	group	group	NOUN
eurjchem-267	33	80	)	)	PUNCT
eurjchem-267	33	81	,	,	PUNCT
eurjchem-267	33	82	135.0	135.0	NUM
eurjchem-267	33	83	,	,	PUNCT
eurjchem-267	33	84	128.3	128.3	NUM
eurjchem-267	33	85	,	,	PUNCT
eurjchem-267	33	86	127.7	127.7	NUM
eurjchem-267	33	87	,	,	PUNCT
eurjchem-267	33	88	128.2	128.2	NUM
eurjchem-267	33	89	(	(	PUNCT
eurjchem-267	33	90	phenyl	phenyl	NOUN
eurjchem-267	33	91	at	at	ADP
eurjchem-267	33	92	c4	c4	NOUN
eurjchem-267	33	93	’	'	PUNCT
eurjchem-267	33	94	)	)	PUNCT
eurjchem-267	33	95	.	.	PUNCT
eurjchem-267	34	1	ms	ms	NOUN
eurjchem-267	34	2	(	(	PUNCT
eurjchem-267	34	3	ei	ei	PROPN
eurjchem-267	34	4	,	,	PUNCT
eurjchem-267	34	5	m	m	PROPN
eurjchem-267	34	6	/	/	SYM
eurjchem-267	34	7	z	z	PROPN
eurjchem-267	34	8	(	(	PUNCT
eurjchem-267	34	9	%	%	NOUN
eurjchem-267	34	10	)	)	PUNCT
eurjchem-267	34	11	):	):	PUNCT
eurjchem-267	34	12	394	394	NUM
eurjchem-267	34	13	(	(	PUNCT
eurjchem-267	34	14	m+	m+	NUM
eurjchem-267	34	15	.	.	PROPN
eurjchem-267	34	16	,	,	PUNCT
eurjchem-267	34	17	22.2	22.2	NUM
eurjchem-267	34	18	)	)	PUNCT
eurjchem-267	34	19	,	,	PUNCT
eurjchem-267	34	20	366	366	NUM
eurjchem-267	34	21	(	(	PUNCT
eurjchem-267	34	22	18.9	18.9	NUM
eurjchem-267	34	23	)	)	PUNCT
eurjchem-267	34	24	,	,	PUNCT
eurjchem-267	34	25	289	289	NUM
eurjchem-267	34	26	(	(	PUNCT
eurjchem-267	34	27	40.3	40.3	NUM
eurjchem-267	34	28	)	)	PUNCT
eurjchem-267	34	29	,	,	PUNCT
eurjchem-267	34	30	147	147	NUM
eurjchem-267	34	31	(	(	PUNCT
eurjchem-267	34	32	100	100	NUM
eurjchem-267	34	33	)	)	PUNCT
eurjchem-267	34	34	,	,	PUNCT
eurjchem-267	34	35	105	105	NUM
eurjchem-267	34	36	(	(	PUNCT
eurjchem-267	34	37	80.2	80.2	NUM
eurjchem-267	34	38	)	)	PUNCT
eurjchem-267	34	39	,	,	PUNCT
eurjchem-267	34	40	77	77	NUM
eurjchem-267	34	41	(	(	PUNCT
eurjchem-267	34	42	36.7	36.7	NUM
eurjchem-267	34	43	)	)	PUNCT
eurjchem-267	34	44	.	.	PUNCT
eurjchem-267	35	1	anal	anal	PROPN
eurjchem-267	35	2	.	.	PUNCT
eurjchem-267	35	3	calcd	calcd	NOUN
eurjchem-267	35	4	.	.	PUNCT
eurjchem-267	36	1	for	for	ADP
eurjchem-267	36	2	c25h18n2o3	c25h18n2o3	PROPN
eurjchem-267	36	3	(	(	PUNCT
eurjchem-267	36	4	394	394	NUM
eurjchem-267	36	5	):	):	PUNCT
eurjchem-267	36	6	c	c	X
eurjchem-267	36	7	,	,	PUNCT
eurjchem-267	36	8	76.14	76.14	NUM
eurjchem-267	36	9	;	;	PUNCT
eurjchem-267	36	10	h	h	NOUN
eurjchem-267	36	11	,	,	PUNCT
eurjchem-267	36	12	4.59	4.59	NUM
eurjchem-267	36	13	;	;	PUNCT
eurjchem-267	36	14	n	n	CCONJ
eurjchem-267	36	15	,	,	PUNCT
eurjchem-267	36	16	7.1	7.1	NUM
eurjchem-267	36	17	.	.	PUNCT
eurjchem-267	36	18	found	find	VERB
eurjchem-267	36	19	:	:	PUNCT
eurjchem-267	37	1	c	c	X
eurjchem-267	37	2	,	,	PUNCT
eurjchem-267	37	3	75.92	75.92	NUM
eurjchem-267	37	4	;	;	PUNCT
eurjchem-267	38	1	h	h	NOUN
eurjchem-267	38	2	,	,	PUNCT
eurjchem-267	38	3	4.66	4.66	NUM
eurjchem-267	38	4	;	;	PUNCT
eurjchem-267	38	5	n	n	CCONJ
eurjchem-267	38	6	,	,	PUNCT
eurjchem-267	38	7	7.06	7.06	NUM
eurjchem-267	38	8	%	%	NOUN
eurjchem-267	38	9	.	.	PUNCT
eurjchem-267	39	1	2.2	2.2	NUM
eurjchem-267	39	2	.	.	PUNCT
eurjchem-267	40	1	2‐[(2z,4e)‐2‐benzamido‐5‐phenylpenta‐2,4‐dienamido]‐	2‐[(2z,4e)‐2‐benzamido‐5‐phenylpenta‐2,4‐dienamido]‐	NUM
eurjchem-267	40	2	n‐p‐tolylbenzamide	n‐p‐tolylbenzamide	NOUN
eurjchem-267	40	3	(	(	PUNCT
eurjchem-267	40	4	2	2	NUM
eurjchem-267	40	5	)	)	PUNCT
eurjchem-267	40	6	method	method	NOUN
eurjchem-267	40	7	1	1	NUM
eurjchem-267	40	8	:	:	PUNCT
eurjchem-267	40	9	to	to	ADP
eurjchem-267	40	10	a	a	DET
eurjchem-267	40	11	solution	solution	NOUN
eurjchem-267	40	12	of	of	ADP
eurjchem-267	40	13	1	1	NUM
eurjchem-267	40	14	(	(	PUNCT
eurjchem-267	40	15	1.2	1.2	NUM
eurjchem-267	40	16	g	g	NOUN
eurjchem-267	40	17	,	,	PUNCT
eurjchem-267	40	18	0.003	0.003	NUM
eurjchem-267	40	19	mol	mol	NOUN
eurjchem-267	40	20	)	)	PUNCT
eurjchem-267	40	21	in	in	ADP
eurjchem-267	40	22	dry	dry	ADJ
eurjchem-267	40	23	benzene	benzene	NOUN
eurjchem-267	40	24	(	(	PUNCT
eurjchem-267	40	25	20	20	NUM
eurjchem-267	40	26	ml	ml	NOUN
eurjchem-267	40	27	)	)	PUNCT
eurjchem-267	40	28	,	,	PUNCT
eurjchem-267	40	29	4‐chlorobenzylidene‐4‐methylaniline	4‐chlorobenzylidene‐4‐methylaniline	NUM
eurjchem-267	40	30	(	(	PUNCT
eurjchem-267	40	31	0.65	0.65	NUM
eurjchem-267	40	32	g	g	NOUN
eurjchem-267	40	33	,	,	PUNCT
eurjchem-267	40	34	mahmoud	mahmoud	PROPN
eurjchem-267	40	35	et	et	PROPN
eurjchem-267	40	36	al	al	PROPN
eurjchem-267	40	37	.	.	PUNCT
eurjchem-267	40	38	/	/	SYM
eurjchem-267	40	39	european	european	PROPN
eurjchem-267	40	40	journal	journal	PROPN
eurjchem-267	40	41	of	of	ADP
eurjchem-267	40	42	chemistry	chemistry	NOUN
eurjchem-267	40	43	2	2	NUM
eurjchem-267	40	44	(	(	PUNCT
eurjchem-267	40	45	3	3	NUM
eurjchem-267	40	46	)	)	PUNCT
eurjchem-267	40	47	(	(	PUNCT
eurjchem-267	40	48	2011	2011	NUM
eurjchem-267	40	49	)	)	PUNCT
eurjchem-267	40	50	404‐409	404‐409	NUM
eurjchem-267	41	1	405	405	NUM
eurjchem-267	41	2	scheme	scheme	NOUN
eurjchem-267	41	3	1	1	NUM
eurjchem-267	41	4	0.003	0.003	NUM
eurjchem-267	41	5	mol	mol	NOUN
eurjchem-267	41	6	)	)	PUNCT
eurjchem-267	41	7	was	be	AUX
eurjchem-267	41	8	added	add	VERB
eurjchem-267	41	9	and	and	CCONJ
eurjchem-267	41	10	then	then	ADV
eurjchem-267	41	11	the	the	DET
eurjchem-267	41	12	reaction	reaction	NOUN
eurjchem-267	41	13	mixture	mixture	NOUN
eurjchem-267	41	14	was	be	AUX
eurjchem-267	41	15	heated	heat	VERB
eurjchem-267	41	16	under	under	ADP
eurjchem-267	41	17	reflux	reflux	NOUN
eurjchem-267	41	18	for	for	ADP
eurjchem-267	41	19	6	6	NUM
eurjchem-267	41	20	hrs	hrs	NOUN
eurjchem-267	41	21	(	(	PUNCT
eurjchem-267	41	22	tlc	tlc	NOUN
eurjchem-267	41	23	)	)	PUNCT
eurjchem-267	41	24	.	.	PUNCT
eurjchem-267	42	1	the	the	DET
eurjchem-267	42	2	solid	solid	ADJ
eurjchem-267	42	3	formed	form	VERB
eurjchem-267	42	4	after	after	SCONJ
eurjchem-267	42	5	cooling	cool	VERB
eurjchem-267	42	6	was	be	AUX
eurjchem-267	42	7	filtered	filter	VERB
eurjchem-267	42	8	off	off	ADP
eurjchem-267	42	9	,	,	PUNCT
eurjchem-267	42	10	dried	dry	VERB
eurjchem-267	42	11	and	and	CCONJ
eurjchem-267	42	12	then	then	ADV
eurjchem-267	42	13	recrystallized	recrystallize	VERB
eurjchem-267	42	14	from	from	ADP
eurjchem-267	42	15	benzene	benzene	NOUN
eurjchem-267	42	16	to	to	PART
eurjchem-267	42	17	give	give	VERB
eurjchem-267	42	18	2	2	NUM
eurjchem-267	42	19	as	as	ADP
eurjchem-267	42	20	yellowish‐white	yellowish‐white	PROPN
eurjchem-267	42	21	crystals	crystal	NOUN
eurjchem-267	42	22	(	(	PUNCT
eurjchem-267	42	23	scheme	scheme	NOUN
eurjchem-267	42	24	1	1	NUM
eurjchem-267	42	25	and	and	CCONJ
eurjchem-267	42	26	2	2	NUM
eurjchem-267	42	27	)	)	PUNCT
eurjchem-267	42	28	.	.	PUNCT
eurjchem-267	43	1	yield	yield	NOUN
eurjchem-267	43	2	:	:	PUNCT
eurjchem-267	43	3	55	55	NUM
eurjchem-267	43	4	%	%	NOUN
eurjchem-267	43	5	.	.	PUNCT
eurjchem-267	44	1	m.p	m.p	PROPN
eurjchem-267	44	2	.	.	PROPN
eurjchem-267	44	3	:	:	PUNCT
eurjchem-267	45	1	176‐178	176‐178	NUM
eurjchem-267	45	2	oc	oc	NOUN
eurjchem-267	45	3	.	.	PUNCT
eurjchem-267	45	4	ft‐ir	ft‐ir	NOUN
eurjchem-267	45	5	(	(	PUNCT
eurjchem-267	45	6	kbr	kbr	PROPN
eurjchem-267	45	7	,	,	PUNCT
eurjchem-267	45	8	cm‐1	cm‐1	PROPN
eurjchem-267	45	9	):	):	PUNCT
eurjchem-267	45	10	3314	3314	NUM
eurjchem-267	45	11	,	,	PUNCT
eurjchem-267	45	12	3216	3216	NUM
eurjchem-267	45	13	ν(nh	ν(nh	NOUN
eurjchem-267	45	14	)	)	PUNCT
eurjchem-267	45	15	,	,	PUNCT
eurjchem-267	45	16	1678	1678	NUM
eurjchem-267	45	17	,	,	PUNCT
eurjchem-267	45	18	1663	1663	NUM
eurjchem-267	45	19	,	,	PUNCT
eurjchem-267	45	20	1658	1658	NUM
eurjchem-267	45	21	ν(c	ν(c	NOUN
eurjchem-267	45	22	=	=	SYM
eurjchem-267	45	23	oamides	oamide	NOUN
eurjchem-267	45	24	)	)	PUNCT
eurjchem-267	45	25	.	.	PUNCT
eurjchem-267	46	1	1h	1h	NUM
eurjchem-267	46	2	nmr	nmr	NOUN
eurjchem-267	46	3	(	(	PUNCT
eurjchem-267	46	4	200	200	NUM
eurjchem-267	46	5	mhz	mhz	NOUN
eurjchem-267	46	6	,	,	PUNCT
eurjchem-267	46	7	cdcl3	cdcl3	NOUN
eurjchem-267	46	8	):	):	PUNCT
eurjchem-267	46	9	10.33	10.33	NUM
eurjchem-267	46	10	(	(	PUNCT
eurjchem-267	46	11	br	br	PROPN
eurjchem-267	46	12	.	.	PUNCT
eurjchem-267	47	1	s.	s.	PROPN
eurjchem-267	47	2	,	,	PUNCT
eurjchem-267	47	3	2h	2h	NUM
eurjchem-267	47	4	,	,	PUNCT
eurjchem-267	47	5	exchangeable	exchangeable	ADJ
eurjchem-267	47	6	with	with	ADP
eurjchem-267	47	7	d2o	d2o	NOUN
eurjchem-267	47	8	)	)	PUNCT
eurjchem-267	47	9	,	,	PUNCT
eurjchem-267	47	10	9.6	9.6	NUM
eurjchem-267	47	11	(	(	PUNCT
eurjchem-267	47	12	s	s	PROPN
eurjchem-267	47	13	,	,	PUNCT
eurjchem-267	47	14	1h	1h	NUM
eurjchem-267	47	15	,	,	PUNCT
eurjchem-267	47	16	exchangeable	exchangeable	ADJ
eurjchem-267	47	17	with	with	ADP
eurjchem-267	47	18	d2o	d2o	NOUN
eurjchem-267	47	19	)	)	PUNCT
eurjchem-267	47	20	,	,	PUNCT
eurjchem-267	47	21	8.4‐7.4	8.4‐7.4	NUM
eurjchem-267	47	22	(	(	PUNCT
eurjchem-267	47	23	m	m	PROPN
eurjchem-267	47	24	,	,	PUNCT
eurjchem-267	47	25	18harom	18harom	NUM
eurjchem-267	47	26	.	.	PUNCT
eurjchem-267	47	27	)	)	PUNCT
eurjchem-267	47	28	,	,	PUNCT
eurjchem-267	48	1	7.1‐6.7	7.1‐6.7	NUM
eurjchem-267	48	2	(	(	PUNCT
eurjchem-267	48	3	m	m	PROPN
eurjchem-267	48	4	,	,	PUNCT
eurjchem-267	48	5	3h	3h	NUM
eurjchem-267	48	6	)	)	PUNCT
eurjchem-267	48	7	,	,	PUNCT
eurjchem-267	48	8	2.3	2.3	NUM
eurjchem-267	48	9	(	(	PUNCT
eurjchem-267	48	10	s	s	PROPN
eurjchem-267	48	11	,	,	PUNCT
eurjchem-267	48	12	3h	3h	NUM
eurjchem-267	48	13	)	)	PUNCT
eurjchem-267	48	14	.	.	PUNCT
eurjchem-267	49	1	ms	ms	NOUN
eurjchem-267	49	2	(	(	PUNCT
eurjchem-267	49	3	ei	ei	PROPN
eurjchem-267	49	4	,	,	PUNCT
eurjchem-267	49	5	m	m	PROPN
eurjchem-267	49	6	/	/	SYM
eurjchem-267	49	7	z	z	PROPN
eurjchem-267	49	8	(	(	PUNCT
eurjchem-267	49	9	%	%	NOUN
eurjchem-267	49	10	)	)	PUNCT
eurjchem-267	49	11	):	):	PUNCT
eurjchem-267	49	12	502	502	NUM
eurjchem-267	49	13	(	(	PUNCT
eurjchem-267	49	14	m+.+1	m+.+1	NOUN
eurjchem-267	49	15	,	,	PUNCT
eurjchem-267	49	16	22.6	22.6	NUM
eurjchem-267	49	17	)	)	PUNCT
eurjchem-267	49	18	,	,	PUNCT
eurjchem-267	49	19	501	501	NUM
eurjchem-267	49	20	(	(	PUNCT
eurjchem-267	49	21	m+	m+	NUM
eurjchem-267	49	22	.	.	PROPN
eurjchem-267	49	23	,	,	PUNCT
eurjchem-267	49	24	100	100	NUM
eurjchem-267	49	25	)	)	PUNCT
eurjchem-267	49	26	,	,	PUNCT
eurjchem-267	49	27	395	395	NUM
eurjchem-267	49	28	(	(	PUNCT
eurjchem-267	49	29	70.1	70.1	NUM
eurjchem-267	49	30	)	)	PUNCT
eurjchem-267	49	31	,	,	PUNCT
eurjchem-267	49	32	276	276	NUM
eurjchem-267	49	33	(	(	PUNCT
eurjchem-267	49	34	16.2	16.2	NUM
eurjchem-267	49	35	)	)	PUNCT
eurjchem-267	49	36	,	,	PUNCT
eurjchem-267	49	37	105	105	NUM
eurjchem-267	49	38	(	(	PUNCT
eurjchem-267	49	39	90.2	90.2	NUM
eurjchem-267	49	40	)	)	PUNCT
eurjchem-267	49	41	,	,	PUNCT
eurjchem-267	49	42	91	91	NUM
eurjchem-267	49	43	(	(	PUNCT
eurjchem-267	49	44	30.1	30.1	NUM
eurjchem-267	49	45	)	)	PUNCT
eurjchem-267	49	46	,	,	PUNCT
eurjchem-267	49	47	77	77	NUM
eurjchem-267	49	48	(	(	PUNCT
eurjchem-267	49	49	76.2	76.2	NUM
eurjchem-267	49	50	)	)	PUNCT
eurjchem-267	49	51	.	.	PUNCT
eurjchem-267	50	1	anal	anal	PROPN
eurjchem-267	50	2	.	.	PUNCT
eurjchem-267	50	3	calcd	calcd	NOUN
eurjchem-267	50	4	.	.	PUNCT
eurjchem-267	51	1	for	for	ADP
eurjchem-267	51	2	c32h27n3o3	c32h27n3o3	NOUN
eurjchem-267	51	3	(	(	PUNCT
eurjchem-267	51	4	501	501	NUM
eurjchem-267	51	5	):	):	PUNCT
eurjchem-267	51	6	c	c	NOUN
eurjchem-267	51	7	,	,	PUNCT
eurjchem-267	51	8	76.64;	76.64;	NOUN
eurjchem-267	51	9	h	h	NOUN
eurjchem-267	51	10	,	,	PUNCT
eurjchem-267	51	11	5.38	5.38	NUM
eurjchem-267	51	12	;	;	PUNCT
eurjchem-267	51	13	n	n	CCONJ
eurjchem-267	51	14	,	,	PUNCT
eurjchem-267	51	15	8.38	8.38	NUM
eurjchem-267	51	16	.	.	PUNCT
eurjchem-267	51	17	found	find	VERB
eurjchem-267	51	18	:	:	PUNCT
eurjchem-267	52	1	c	c	X
eurjchem-267	52	2	,	,	PUNCT
eurjchem-267	52	3	76.34	76.34	NUM
eurjchem-267	52	4	;	;	PUNCT
eurjchem-267	52	5	h	h	X
eurjchem-267	52	6	,	,	PUNCT
eurjchem-267	52	7	5.22	5.22	NUM
eurjchem-267	52	8	;	;	PUNCT
eurjchem-267	52	9	n	n	CCONJ
eurjchem-267	52	10	,	,	PUNCT
eurjchem-267	52	11	8.75	8.75	NUM
eurjchem-267	52	12	%	%	NOUN
eurjchem-267	52	13	.	.	PUNCT
eurjchem-267	53	1	method	method	NOUN
eurjchem-267	53	2	2	2	NUM
eurjchem-267	53	3	:	:	SYM
eurjchem-267	53	4	p‐toluidine	p‐toluidine	X
eurjchem-267	53	5	(	(	PUNCT
eurjchem-267	53	6	0.32	0.32	NUM
eurjchem-267	53	7	g	g	NOUN
eurjchem-267	53	8	,	,	PUNCT
eurjchem-267	53	9	0.003	0.003	NUM
eurjchem-267	53	10	mol	mol	NOUN
eurjchem-267	53	11	)	)	PUNCT
eurjchem-267	53	12	was	be	AUX
eurjchem-267	53	13	added	add	VERB
eurjchem-267	53	14	to	to	ADP
eurjchem-267	53	15	a	a	DET
eurjchem-267	53	16	stirred	stir	VERB
eurjchem-267	53	17	solution	solution	NOUN
eurjchem-267	53	18	of	of	ADP
eurjchem-267	53	19	1	1	NUM
eurjchem-267	53	20	(	(	PUNCT
eurjchem-267	53	21	1.2	1.2	NUM
eurjchem-267	53	22	g	g	NOUN
eurjchem-267	53	23	,	,	PUNCT
eurjchem-267	53	24	0.003	0.003	NUM
eurjchem-267	53	25	mol	mol	NOUN
eurjchem-267	53	26	)	)	PUNCT
eurjchem-267	53	27	in	in	ADP
eurjchem-267	53	28	ethanol	ethanol	NOUN
eurjchem-267	53	29	(	(	PUNCT
eurjchem-267	53	30	20	20	NUM
eurjchem-267	53	31	ml	ml	NOUN
eurjchem-267	53	32	)	)	PUNCT
eurjchem-267	53	33	and	and	CCONJ
eurjchem-267	53	34	the	the	DET
eurjchem-267	53	35	reaction	reaction	NOUN
eurjchem-267	53	36	mixture	mixture	NOUN
eurjchem-267	53	37	was	be	AUX
eurjchem-267	53	38	refluxed	refluxe	VERB
eurjchem-267	53	39	for	for	ADP
eurjchem-267	53	40	2	2	NUM
eurjchem-267	53	41	hrs	hrs	NOUN
eurjchem-267	53	42	(	(	PUNCT
eurjchem-267	53	43	tlc	tlc	NOUN
eurjchem-267	53	44	)	)	PUNCT
eurjchem-267	53	45	.	.	PUNCT
eurjchem-267	54	1	evaporation	evaporation	NOUN
eurjchem-267	54	2	of	of	ADP
eurjchem-267	54	3	the	the	DET
eurjchem-267	54	4	excess	excess	ADJ
eurjchem-267	54	5	ethanol	ethanol	NOUN
eurjchem-267	54	6	left	leave	VERB
eurjchem-267	54	7	a	a	DET
eurjchem-267	54	8	crude	crude	ADJ
eurjchem-267	54	9	pale	pale	ADJ
eurjchem-267	54	10	yellow	yellow	ADJ
eurjchem-267	54	11	product	product	NOUN
eurjchem-267	54	12	which	which	PRON
eurjchem-267	54	13	recrystallized	recrystallize	VERB
eurjchem-267	54	14	from	from	ADP
eurjchem-267	54	15	benzene	benzene	NOUN
eurjchem-267	54	16	to	to	PART
eurjchem-267	54	17	give	give	VERB
eurjchem-267	54	18	2	2	NUM
eurjchem-267	54	19	;	;	PUNCT
eurjchem-267	54	20	yield	yield	VERB
eurjchem-267	54	21	86.3	86.3	NUM
eurjchem-267	54	22	%	%	NOUN
eurjchem-267	54	23	(	(	PUNCT
eurjchem-267	54	24	identity	identity	NOUN
eurjchem-267	54	25	m.p	m.p	PROPN
eurjchem-267	54	26	,	,	PUNCT
eurjchem-267	54	27	mixed	mixed	ADJ
eurjchem-267	54	28	m.p	m.p	PROPN
eurjchem-267	54	29	,	,	PUNCT
eurjchem-267	54	30	tlc	tlc	NOUN
eurjchem-267	54	31	)	)	PUNCT
eurjchem-267	54	32	.	.	PUNCT
eurjchem-267	55	1	2.3	2.3	NUM
eurjchem-267	55	2	.	.	NUM
eurjchem-267	55	3	2‐[(1z,3e)‐1‐benzamido‐4‐phenyl‐1,3‐butadien‐1‐yl]‐3‐	2‐[(1z,3e)‐1‐benzamido‐4‐phenyl‐1,3‐butadien‐1‐yl]‐3‐	NUM
eurjchem-267	55	4	(	(	PUNCT
eurjchem-267	55	5	4‐methylphenyl	4‐methylphenyl	NUM
eurjchem-267	55	6	)	)	PUNCT
eurjchem-267	55	7	quinazolin‐4(h)‐one	quinazolin‐4(h)‐one	PROPN
eurjchem-267	55	8	(	(	PUNCT
eurjchem-267	55	9	3	3	NUM
eurjchem-267	55	10	)	)	PUNCT
eurjchem-267	55	11	method	method	NOUN
eurjchem-267	55	12	1	1	NUM
eurjchem-267	55	13	:	:	PUNCT
eurjchem-267	55	14	a	a	DET
eurjchem-267	55	15	mixture	mixture	NOUN
eurjchem-267	55	16	of	of	ADP
eurjchem-267	55	17	1	1	NUM
eurjchem-267	55	18	(	(	PUNCT
eurjchem-267	55	19	3.49	3.49	NUM
eurjchem-267	55	20	g	g	NOUN
eurjchem-267	55	21	,	,	PUNCT
eurjchem-267	55	22	0.01	0.01	NUM
eurjchem-267	55	23	mol	mol	NOUN
eurjchem-267	55	24	)	)	PUNCT
eurjchem-267	55	25	,	,	PUNCT
eurjchem-267	55	26	schiff	schiff	NOUN
eurjchem-267	55	27	’s	’s	PART
eurjchem-267	55	28	base	base	NOUN
eurjchem-267	55	29	(	(	PUNCT
eurjchem-267	55	30	4‐	4‐	PROPN
eurjchem-267	55	31	chlorobenzylidene‐4‐methylaniline	chlorobenzylidene‐4‐methylaniline	NUM
eurjchem-267	55	32	)	)	PUNCT
eurjchem-267	55	33	(	(	PUNCT
eurjchem-267	55	34	2.3	2.3	NUM
eurjchem-267	55	35	g	g	NOUN
eurjchem-267	55	36	,	,	PUNCT
eurjchem-267	55	37	0.01	0.01	NUM
eurjchem-267	55	38	mol	mol	NOUN
eurjchem-267	55	39	)	)	PUNCT
eurjchem-267	55	40	and	and	CCONJ
eurjchem-267	55	41	anhydrous	anhydrous	ADJ
eurjchem-267	55	42	sodium	sodium	NOUN
eurjchem-267	55	43	acetate	acetate	NOUN
eurjchem-267	55	44	(	(	PUNCT
eurjchem-267	55	45	2	2	NUM
eurjchem-267	55	46	g	g	NOUN
eurjchem-267	55	47	,	,	PUNCT
eurjchem-267	55	48	0.024	0.024	NUM
eurjchem-267	55	49	mol	mol	NOUN
eurjchem-267	55	50	)	)	PUNCT
eurjchem-267	55	51	in	in	ADP
eurjchem-267	55	52	acetic	acetic	ADJ
eurjchem-267	55	53	acid	acid	NOUN
eurjchem-267	55	54	(	(	PUNCT
eurjchem-267	55	55	30	30	NUM
eurjchem-267	55	56	ml	ml	NOUN
eurjchem-267	55	57	)	)	PUNCT
eurjchem-267	55	58	was	be	AUX
eurjchem-267	55	59	heated	heat	VERB
eurjchem-267	55	60	under	under	ADP
eurjchem-267	55	61	reflux	reflux	NOUN
eurjchem-267	55	62	for	for	ADP
eurjchem-267	55	63	6	6	NUM
eurjchem-267	55	64	hrs	hrs	NOUN
eurjchem-267	55	65	,	,	PUNCT
eurjchem-267	55	66	then	then	ADV
eurjchem-267	55	67	the	the	DET
eurjchem-267	55	68	reaction	reaction	NOUN
eurjchem-267	55	69	mixture	mixture	NOUN
eurjchem-267	55	70	was	be	AUX
eurjchem-267	55	71	allowed	allow	VERB
eurjchem-267	55	72	to	to	PART
eurjchem-267	55	73	cool	cool	VERB
eurjchem-267	55	74	.	.	PUNCT
eurjchem-267	56	1	the	the	DET
eurjchem-267	56	2	cooled	cool	VERB
eurjchem-267	56	3	mixture	mixture	NOUN
eurjchem-267	56	4	was	be	AUX
eurjchem-267	56	5	stirred	stir	VERB
eurjchem-267	56	6	with	with	ADP
eurjchem-267	56	7	water	water	NOUN
eurjchem-267	56	8	(	(	PUNCT
eurjchem-267	56	9	100	100	NUM
eurjchem-267	56	10	ml	ml	NOUN
eurjchem-267	56	11	)	)	PUNCT
eurjchem-267	56	12	for	for	ADP
eurjchem-267	56	13	15	15	NUM
eurjchem-267	56	14	min	min	NOUN
eurjchem-267	56	15	.	.	PROPN
eurjchem-267	56	16	and	and	CCONJ
eurjchem-267	56	17	the	the	DET
eurjchem-267	56	18	solid	solid	ADJ
eurjchem-267	56	19	formed	form	VERB
eurjchem-267	56	20	was	be	AUX
eurjchem-267	56	21	filtered	filter	VERB
eurjchem-267	56	22	off	off	ADP
eurjchem-267	56	23	,	,	PUNCT
eurjchem-267	56	24	dried	dry	VERB
eurjchem-267	56	25	and	and	CCONJ
eurjchem-267	56	26	recrystallized	recrystallize	VERB
eurjchem-267	56	27	from	from	ADP
eurjchem-267	56	28	ethanol	ethanol	NOUN
eurjchem-267	56	29	to	to	PART
eurjchem-267	56	30	give	give	VERB
eurjchem-267	56	31	3	3	NUM
eurjchem-267	56	32	as	as	ADP
eurjchem-267	56	33	orange	orange	ADJ
eurjchem-267	56	34	crystals	crystal	NOUN
eurjchem-267	56	35	(	(	PUNCT
eurjchem-267	56	36	scheme	scheme	NOUN
eurjchem-267	56	37	1	1	NUM
eurjchem-267	56	38	and	and	CCONJ
eurjchem-267	56	39	2	2	NUM
eurjchem-267	56	40	)	)	PUNCT
eurjchem-267	56	41	.	.	PUNCT
eurjchem-267	57	1	yield	yield	NOUN
eurjchem-267	57	2	:	:	PUNCT
eurjchem-267	57	3	55	55	NUM
eurjchem-267	57	4	%	%	NOUN
eurjchem-267	57	5	.	.	PUNCT
eurjchem-267	58	1	m.p.:127‐129	m.p.:127‐129	PROPN
eurjchem-267	58	2	oc	oc	PROPN
eurjchem-267	58	3	.	.	PUNCT
eurjchem-267	59	1	ft‐ir	ft‐ir	NOUN
eurjchem-267	59	2	(	(	PUNCT
eurjchem-267	59	3	kbr	kbr	PROPN
eurjchem-267	59	4	,	,	PUNCT
eurjchem-267	59	5	cm‐1	cm‐1	PROPN
eurjchem-267	59	6	):	):	PUNCT
eurjchem-267	59	7	3278	3278	NUM
eurjchem-267	59	8	ν(nh	ν(nh	NOUN
eurjchem-267	59	9	)	)	PUNCT
eurjchem-267	59	10	,	,	PUNCT
eurjchem-267	59	11	1722	1722	NUM
eurjchem-267	59	12	ν(c	ν(c	PROPN
eurjchem-267	59	13	=	=	SYM
eurjchem-267	59	14	o	o	NOUN
eurjchem-267	59	15	)	)	PUNCT
eurjchem-267	59	16	,	,	PUNCT
eurjchem-267	59	17	1650	1650	NUM
eurjchem-267	59	18	ν(c	ν(c	NOUN
eurjchem-267	59	19	=	=	SYM
eurjchem-267	59	20	oamide	oamide	ADV
eurjchem-267	59	21	)	)	PUNCT
eurjchem-267	59	22	,	,	PUNCT
eurjchem-267	59	23	1632	1632	NUM
eurjchem-267	59	24	ν(c	ν(c	PROPN
eurjchem-267	59	25	=	=	SYM
eurjchem-267	59	26	n	n	CCONJ
eurjchem-267	59	27	)	)	PUNCT
eurjchem-267	59	28	.	.	PUNCT
eurjchem-267	60	1	1h	1h	NUM
eurjchem-267	60	2	nmr	nmr	NOUN
eurjchem-267	60	3	(	(	PUNCT
eurjchem-267	60	4	200	200	NUM
eurjchem-267	60	5	mhz	mhz	NOUN
eurjchem-267	60	6	,	,	PUNCT
eurjchem-267	60	7	cdcl3	cdcl3	NOUN
eurjchem-267	60	8	):	):	PUNCT
eurjchem-267	60	9	9.4	9.4	NUM
eurjchem-267	60	10	(	(	PUNCT
eurjchem-267	60	11	s	s	PROPN
eurjchem-267	60	12	,	,	PUNCT
eurjchem-267	60	13	1h	1h	NUM
eurjchem-267	60	14	,	,	PUNCT
eurjchem-267	60	15	exchangeable	exchangeable	ADJ
eurjchem-267	60	16	with	with	ADP
eurjchem-267	60	17	d2o	d2o	NOUN
eurjchem-267	60	18	)	)	PUNCT
eurjchem-267	60	19	,	,	PUNCT
eurjchem-267	60	20	8.5‐7.3	8.5‐7.3	ADP
eurjchem-267	60	21	(	(	PUNCT
eurjchem-267	60	22	m	m	PROPN
eurjchem-267	60	23	,	,	PUNCT
eurjchem-267	60	24	18harom	18harom	NUM
eurjchem-267	60	25	.	.	PUNCT
eurjchem-267	60	26	)	)	PUNCT
eurjchem-267	60	27	,	,	PUNCT
eurjchem-267	60	28	7.1‐6.6	7.1‐6.6	NUM
eurjchem-267	60	29	(	(	PUNCT
eurjchem-267	60	30	m	m	PROPN
eurjchem-267	60	31	,	,	PUNCT
eurjchem-267	60	32	3h	3h	NUM
eurjchem-267	60	33	)	)	PUNCT
eurjchem-267	60	34	,	,	PUNCT
eurjchem-267	60	35	2.3	2.3	NUM
eurjchem-267	60	36	(	(	PUNCT
eurjchem-267	60	37	s	s	PROPN
eurjchem-267	60	38	,	,	PUNCT
eurjchem-267	60	39	3h	3h	NUM
eurjchem-267	60	40	)	)	PUNCT
eurjchem-267	60	41	.	.	PUNCT
eurjchem-267	61	1	13c	13c	NOUN
eurjchem-267	61	2	nmr	nmr	NOUN
eurjchem-267	61	3	(	(	PUNCT
eurjchem-267	61	4	200	200	NUM
eurjchem-267	61	5	mhz	mhz	NOUN
eurjchem-267	61	6	,	,	PUNCT
eurjchem-267	61	7	cdcl3	cdcl3	NOUN
eurjchem-267	61	8	):	):	PUNCT
eurjchem-267	61	9	167.8	167.8	NUM
eurjchem-267	61	10	(	(	PUNCT
eurjchem-267	61	11	coamide	coamide	ADJ
eurjchem-267	61	12	)	)	PUNCT
eurjchem-267	61	13	,	,	PUNCT
eurjchem-267	61	14	163.4	163.4	NUM
eurjchem-267	61	15	(	(	PUNCT
eurjchem-267	61	16	co	co	NOUN
eurjchem-267	61	17	)	)	PUNCT
eurjchem-267	61	18	,	,	PUNCT
eurjchem-267	61	19	159.6	159.6	NUM
eurjchem-267	61	20	(	(	PUNCT
eurjchem-267	61	21	c2	c2	PROPN
eurjchem-267	61	22	)	)	PUNCT
eurjchem-267	61	23	,	,	PUNCT
eurjchem-267	61	24	138.1	138.1	NUM
eurjchem-267	61	25	,	,	PUNCT
eurjchem-267	61	26	123.6	123.6	NUM
eurjchem-267	61	27	,	,	PUNCT
eurjchem-267	61	28	122.3	122.3	NUM
eurjchem-267	61	29	,	,	PUNCT
eurjchem-267	61	30	110.2	110.2	NUM
eurjchem-267	61	31	(	(	PUNCT
eurjchem-267	61	32	c1‐	c1‐	NOUN
eurjchem-267	61	33	c4butadiene	c4butadiene	PROPN
eurjchem-267	61	34	)	)	PUNCT
eurjchem-267	61	35	,	,	PUNCT
eurjchem-267	61	36	21.4	21.4	NUM
eurjchem-267	61	37	(	(	PUNCT
eurjchem-267	61	38	ch3	ch3	PROPN
eurjchem-267	61	39	)	)	PUNCT
eurjchem-267	61	40	,	,	PUNCT
eurjchem-267	61	41	135.6	135.6	NUM
eurjchem-267	61	42	,	,	PUNCT
eurjchem-267	61	43	129.7	129.7	NUM
eurjchem-267	61	44	,	,	PUNCT
eurjchem-267	61	45	128.5	128.5	NUM
eurjchem-267	61	46	,	,	PUNCT
eurjchem-267	61	47	127.9	127.9	NUM
eurjchem-267	61	48	(	(	PUNCT
eurjchem-267	61	49	p‐tolyl	p‐tolyl	NUM
eurjchem-267	61	50	)	)	PUNCT
eurjchem-267	61	51	,	,	PUNCT
eurjchem-267	61	52	135.2	135.2	NUM
eurjchem-267	61	53	,	,	PUNCT
eurjchem-267	61	54	128.6	128.6	NUM
eurjchem-267	61	55	,	,	PUNCT
eurjchem-267	61	56	128.5	128.5	NUM
eurjchem-267	61	57	,	,	PUNCT
eurjchem-267	61	58	128.1	128.1	NUM
eurjchem-267	61	59	,	,	PUNCT
eurjchem-267	61	60	126.9	126.9	NUM
eurjchem-267	61	61	(	(	PUNCT
eurjchem-267	61	62	c4‐	c4‐	NOUN
eurjchem-267	61	63	phenyl	phenyl	NOUN
eurjchem-267	61	64	)	)	PUNCT
eurjchem-267	61	65	,	,	PUNCT
eurjchem-267	61	66	133.2	133.2	NUM
eurjchem-267	61	67	,	,	PUNCT
eurjchem-267	61	68	132.1	132.1	NUM
eurjchem-267	61	69	,	,	PUNCT
eurjchem-267	61	70	128.1	128.1	NUM
eurjchem-267	61	71	,	,	PUNCT
eurjchem-267	61	72	127.5	127.5	NUM
eurjchem-267	61	73	(	(	PUNCT
eurjchem-267	61	74	phenyl	phenyl	NOUN
eurjchem-267	61	75	ring	ring	NOUN
eurjchem-267	61	76	of	of	ADP
eurjchem-267	61	77	benzamido	benzamido	ADJ
eurjchem-267	61	78	group	group	NOUN
eurjchem-267	61	79	)	)	PUNCT
eurjchem-267	61	80	.	.	PUNCT
eurjchem-267	62	1	ms	ms	NOUN
eurjchem-267	62	2	(	(	PUNCT
eurjchem-267	62	3	ei	ei	PROPN
eurjchem-267	62	4	,	,	PUNCT
eurjchem-267	62	5	m	m	PROPN
eurjchem-267	62	6	/	/	SYM
eurjchem-267	62	7	z	z	PROPN
eurjchem-267	62	8	(	(	PUNCT
eurjchem-267	62	9	%	%	NOUN
eurjchem-267	62	10	)	)	PUNCT
eurjchem-267	62	11	):	):	PUNCT
eurjchem-267	62	12	483	483	NUM
eurjchem-267	62	13	(	(	PUNCT
eurjchem-267	62	14	m+	m+	NUM
eurjchem-267	62	15	.	.	PROPN
eurjchem-267	62	16	,	,	PUNCT
eurjchem-267	62	17	70.3	70.3	NUM
eurjchem-267	62	18	)	)	PUNCT
eurjchem-267	62	19	,	,	PUNCT
eurjchem-267	62	20	393	393	NUM
eurjchem-267	62	21	(	(	PUNCT
eurjchem-267	62	22	18.6	18.6	NUM
eurjchem-267	62	23	)	)	PUNCT
eurjchem-267	62	24	,	,	PUNCT
eurjchem-267	62	25	236	236	NUM
eurjchem-267	62	26	(	(	PUNCT
eurjchem-267	62	27	66.3	66.3	NUM
eurjchem-267	62	28	)	)	PUNCT
eurjchem-267	62	29	,	,	PUNCT
eurjchem-267	62	30	105	105	NUM
eurjchem-267	62	31	(	(	PUNCT
eurjchem-267	62	32	100	100	NUM
eurjchem-267	62	33	)	)	PUNCT
eurjchem-267	62	34	,	,	PUNCT
eurjchem-267	62	35	77	77	NUM
eurjchem-267	62	36	(	(	PUNCT
eurjchem-267	62	37	46.2	46.2	NUM
eurjchem-267	62	38	)	)	PUNCT
eurjchem-267	62	39	.	.	PUNCT
eurjchem-267	63	1	anal	anal	PROPN
eurjchem-267	63	2	.	.	PUNCT
eurjchem-267	63	3	calcd	calcd	NOUN
eurjchem-267	63	4	.	.	PUNCT
eurjchem-267	64	1	for	for	ADP
eurjchem-267	64	2	c32h25n3o2	c32h25n3o2	PROPN
eurjchem-267	64	3	(	(	PUNCT
eurjchem-267	64	4	483	483	NUM
eurjchem-267	64	5	):	):	PUNCT
eurjchem-267	64	6	c	c	NOUN
eurjchem-267	64	7	,	,	PUNCT
eurjchem-267	64	8	79.50;	79.50;	NUM
eurjchem-267	64	9	h	h	NOUN
eurjchem-267	64	10	,	,	PUNCT
eurjchem-267	64	11	5.17	5.17	NUM
eurjchem-267	64	12	;	;	PUNCT
eurjchem-267	64	13	n	n	CCONJ
eurjchem-267	64	14	,	,	PUNCT
eurjchem-267	64	15	8.69	8.69	NUM
eurjchem-267	64	16	.	.	PUNCT
eurjchem-267	64	17	found	find	VERB
eurjchem-267	64	18	:	:	PUNCT
eurjchem-267	65	1	c	c	X
eurjchem-267	65	2	,	,	PUNCT
eurjchem-267	65	3	79.34	79.34	NUM
eurjchem-267	65	4	;	;	PUNCT
eurjchem-267	65	5	h	h	NOUN
eurjchem-267	65	6	,	,	PUNCT
eurjchem-267	65	7	5.32	5.32	NUM
eurjchem-267	65	8	;	;	PUNCT
eurjchem-267	65	9	n	n	CCONJ
eurjchem-267	65	10	,	,	PUNCT
eurjchem-267	65	11	8.45	8.45	NUM
eurjchem-267	65	12	%	%	NOUN
eurjchem-267	65	13	.	.	PUNCT
eurjchem-267	66	1	method	method	NOUN
eurjchem-267	66	2	2	2	NUM
eurjchem-267	66	3	:	:	PUNCT
eurjchem-267	66	4	compound	compound	NOUN
eurjchem-267	66	5	1	1	NUM
eurjchem-267	66	6	(	(	PUNCT
eurjchem-267	66	7	1.2	1.2	NUM
eurjchem-267	66	8	g	g	NOUN
eurjchem-267	66	9	,	,	PUNCT
eurjchem-267	66	10	0.003	0.003	NUM
eurjchem-267	66	11	mol	mol	NOUN
eurjchem-267	66	12	)	)	PUNCT
eurjchem-267	66	13	was	be	AUX
eurjchem-267	66	14	heated	heat	VERB
eurjchem-267	66	15	with	with	ADP
eurjchem-267	66	16	p‐toluidine	p‐toluidine	PUNCT
eurjchem-267	66	17	(	(	PUNCT
eurjchem-267	66	18	0.32	0.32	NUM
eurjchem-267	66	19	g	g	NOUN
eurjchem-267	66	20	,	,	PUNCT
eurjchem-267	66	21	0.003	0.003	NUM
eurjchem-267	66	22	mol	mol	NOUN
eurjchem-267	66	23	)	)	PUNCT
eurjchem-267	66	24	in	in	ADP
eurjchem-267	66	25	refluxing	refluxing	NOUN
eurjchem-267	66	26	n‐butanol	n‐butanol	PUNCT
eurjchem-267	66	27	(	(	PUNCT
eurjchem-267	66	28	20	20	NUM
eurjchem-267	66	29	ml	ml	NOUN
eurjchem-267	66	30	)	)	PUNCT
eurjchem-267	66	31	for	for	ADP
eurjchem-267	66	32	10	10	NUM
eurjchem-267	66	33	hrs	hrs	NOUN
eurjchem-267	66	34	(	(	PUNCT
eurjchem-267	66	35	tlc	tlc	NOUN
eurjchem-267	66	36	)	)	PUNCT
eurjchem-267	66	37	.	.	PUNCT
eurjchem-267	67	1	the	the	DET
eurjchem-267	67	2	reaction	reaction	NOUN
eurjchem-267	67	3	mixture	mixture	NOUN
eurjchem-267	67	4	was	be	AUX
eurjchem-267	67	5	concentrated	concentrate	VERB
eurjchem-267	67	6	and	and	CCONJ
eurjchem-267	67	7	the	the	DET
eurjchem-267	67	8	deposited	deposit	VERB
eurjchem-267	67	9	solid	solid	ADJ
eurjchem-267	67	10	after	after	SCONJ
eurjchem-267	67	11	cooling	cool	VERB
eurjchem-267	67	12	was	be	AUX
eurjchem-267	67	13	collected	collect	VERB
eurjchem-267	67	14	by	by	ADP
eurjchem-267	67	15	filtration	filtration	NOUN
eurjchem-267	67	16	and	and	CCONJ
eurjchem-267	67	17	recrystallized	recrystallize	VERB
eurjchem-267	67	18	from	from	ADP
eurjchem-267	67	19	ethanol	ethanol	NOUN
eurjchem-267	67	20	to	to	PART
eurjchem-267	67	21	give	give	VERB
eurjchem-267	67	22	3	3	NUM
eurjchem-267	67	23	;	;	PUNCT
eurjchem-267	67	24	yield	yield	VERB
eurjchem-267	67	25	64	64	NUM
eurjchem-267	67	26	%	%	NOUN
eurjchem-267	67	27	(	(	PUNCT
eurjchem-267	67	28	identity	identity	NOUN
eurjchem-267	67	29	m.p	m.p	PROPN
eurjchem-267	67	30	,	,	PUNCT
eurjchem-267	67	31	mixed	mixed	ADJ
eurjchem-267	67	32	m.p	m.p	PROPN
eurjchem-267	67	33	,	,	PUNCT
eurjchem-267	67	34	tlc	tlc	NOUN
eurjchem-267	67	35	,	,	PUNCT
eurjchem-267	67	36	ir	ir	PROPN
eurjchem-267	67	37	)	)	PUNCT
eurjchem-267	67	38	.	.	PUNCT
eurjchem-267	68	1	406	406	NUM
eurjchem-267	68	2	mahmoud	mahmoud	PROPN
eurjchem-267	68	3	et	et	PROPN
eurjchem-267	68	4	al	al	PROPN
eurjchem-267	68	5	.	.	PUNCT
eurjchem-267	68	6	/	/	SYM
eurjchem-267	68	7	european	european	PROPN
eurjchem-267	68	8	journal	journal	PROPN
eurjchem-267	68	9	of	of	ADP
eurjchem-267	68	10	chemistry	chemistry	NOUN
eurjchem-267	68	11	2	2	NUM
eurjchem-267	68	12	(	(	PUNCT
eurjchem-267	68	13	3	3	NUM
eurjchem-267	68	14	)	)	PUNCT
eurjchem-267	68	15	(	(	PUNCT
eurjchem-267	68	16	2011	2011	NUM
eurjchem-267	68	17	)	)	PUNCT
eurjchem-267	68	18	404‐409	404‐409	NUM
eurjchem-267	68	19	scheme	scheme	NOUN
eurjchem-267	68	20	2	2	NUM
eurjchem-267	68	21	method	method	NOUN
eurjchem-267	68	22	3	3	NUM
eurjchem-267	68	23	:	:	PUNCT
eurjchem-267	68	24	compound	compound	NOUN
eurjchem-267	68	25	2	2	NUM
eurjchem-267	68	26	(	(	PUNCT
eurjchem-267	68	27	1.5	1.5	NUM
eurjchem-267	68	28	g	g	NOUN
eurjchem-267	68	29	,	,	PUNCT
eurjchem-267	68	30	0.003	0.003	NUM
eurjchem-267	68	31	mol	mol	NOUN
eurjchem-267	68	32	)	)	PUNCT
eurjchem-267	68	33	was	be	AUX
eurjchem-267	68	34	heated	heat	VERB
eurjchem-267	68	35	on	on	ADP
eurjchem-267	68	36	an	an	DET
eurjchem-267	68	37	oil‐bath	oil‐bath	NOUN
eurjchem-267	68	38	at	at	ADP
eurjchem-267	68	39	200	200	NUM
eurjchem-267	68	40	oc	oc	NOUN
eurjchem-267	68	41	for	for	ADP
eurjchem-267	68	42	1	1	NUM
eurjchem-267	68	43	hr	hr	NOUN
eurjchem-267	68	44	and	and	CCONJ
eurjchem-267	68	45	left	leave	VERB
eurjchem-267	68	46	at	at	ADP
eurjchem-267	68	47	room	room	NOUN
eurjchem-267	68	48	temperature	temperature	NOUN
eurjchem-267	68	49	to	to	PART
eurjchem-267	68	50	cool	cool	VERB
eurjchem-267	68	51	.	.	PUNCT
eurjchem-267	69	1	the	the	DET
eurjchem-267	69	2	resulting	result	VERB
eurjchem-267	69	3	melt	melt	NOUN
eurjchem-267	69	4	was	be	AUX
eurjchem-267	69	5	triturated	triturate	VERB
eurjchem-267	69	6	with	with	ADP
eurjchem-267	69	7	boiling	boiling	NOUN
eurjchem-267	69	8	ethanol	ethanol	NOUN
eurjchem-267	69	9	and	and	CCONJ
eurjchem-267	69	10	concentrated	concentrate	VERB
eurjchem-267	69	11	then	then	ADV
eurjchem-267	69	12	left	leave	VERB
eurjchem-267	69	13	to	to	PART
eurjchem-267	69	14	cool	cool	ADJ
eurjchem-267	69	15	.	.	PUNCT
eurjchem-267	70	1	the	the	DET
eurjchem-267	70	2	solid	solid	ADJ
eurjchem-267	70	3	formed	form	VERB
eurjchem-267	70	4	was	be	AUX
eurjchem-267	70	5	filtered	filter	VERB
eurjchem-267	70	6	off	off	ADP
eurjchem-267	70	7	,	,	PUNCT
eurjchem-267	70	8	dried	dry	VERB
eurjchem-267	70	9	and	and	CCONJ
eurjchem-267	70	10	recrystallized	recrystallize	VERB
eurjchem-267	70	11	from	from	ADP
eurjchem-267	70	12	ethanol	ethanol	NOUN
eurjchem-267	70	13	to	to	PART
eurjchem-267	70	14	give	give	VERB
eurjchem-267	70	15	3	3	NUM
eurjchem-267	70	16	as	as	ADP
eurjchem-267	70	17	orange	orange	ADJ
eurjchem-267	70	18	crystals	crystal	NOUN
eurjchem-267	70	19	;	;	PUNCT
eurjchem-267	70	20	yield	yield	VERB
eurjchem-267	70	21	71	71	NUM
eurjchem-267	70	22	%	%	NOUN
eurjchem-267	70	23	,	,	PUNCT
eurjchem-267	70	24	which	which	PRON
eurjchem-267	70	25	show	show	VERB
eurjchem-267	70	26	no	no	DET
eurjchem-267	70	27	depression	depression	NOUN
eurjchem-267	70	28	when	when	SCONJ
eurjchem-267	70	29	admixed	admix	VERB
eurjchem-267	70	30	with	with	ADP
eurjchem-267	70	31	3	3	NUM
eurjchem-267	70	32	.	.	NOUN
eurjchem-267	70	33	2.4	2.4	NUM
eurjchem-267	70	34	.	.	PUNCT
eurjchem-267	71	1	3‐(4‐chlorobenzylidene)amino‐2‐[(1z,3e)‐1‐benzamido‐	3‐(4‐chlorobenzylidene)amino‐2‐[(1z,3e)‐1‐benzamido‐	NUM
eurjchem-267	71	2	4‐phenyl‐1,3‐butadien‐1‐yl]quinazolin‐4(h)‐one	4‐phenyl‐1,3‐butadien‐1‐yl]quinazolin‐4(h)‐one	NOUN
eurjchem-267	71	3	(	(	PUNCT
eurjchem-267	71	4	4	4	NUM
eurjchem-267	71	5	)	)	PUNCT
eurjchem-267	71	6	a	a	DET
eurjchem-267	71	7	mixture	mixture	NOUN
eurjchem-267	71	8	of	of	ADP
eurjchem-267	71	9	1	1	NUM
eurjchem-267	71	10	(	(	PUNCT
eurjchem-267	71	11	0.01	0.01	NUM
eurjchem-267	71	12	mol	mol	NOUN
eurjchem-267	71	13	)	)	PUNCT
eurjchem-267	71	14	,	,	PUNCT
eurjchem-267	71	15	4‐chlorobenzalazine	4‐chlorobenzalazine	NUM
eurjchem-267	71	16	(	(	PUNCT
eurjchem-267	71	17	2.76	2.76	NUM
eurjchem-267	71	18	g	g	NOUN
eurjchem-267	71	19	,	,	PUNCT
eurjchem-267	71	20	0.01	0.01	NUM
eurjchem-267	71	21	mol	mol	NOUN
eurjchem-267	71	22	)	)	PUNCT
eurjchem-267	71	23	and	and	CCONJ
eurjchem-267	71	24	anhydrous	anhydrous	ADJ
eurjchem-267	71	25	sodium	sodium	NOUN
eurjchem-267	71	26	acetate	acetate	NOUN
eurjchem-267	71	27	(	(	PUNCT
eurjchem-267	71	28	2	2	NUM
eurjchem-267	71	29	g	g	NOUN
eurjchem-267	71	30	)	)	PUNCT
eurjchem-267	71	31	in	in	ADP
eurjchem-267	71	32	glacial	glacial	ADJ
eurjchem-267	71	33	acetic	acetic	ADJ
eurjchem-267	71	34	acid	acid	NOUN
eurjchem-267	71	35	was	be	AUX
eurjchem-267	71	36	heated	heat	VERB
eurjchem-267	71	37	under	under	ADP
eurjchem-267	71	38	reflux	reflux	NOUN
eurjchem-267	71	39	for	for	ADP
eurjchem-267	71	40	10	10	NUM
eurjchem-267	71	41	hrs	hrs	NOUN
eurjchem-267	71	42	(	(	PUNCT
eurjchem-267	71	43	tlc	tlc	NOUN
eurjchem-267	71	44	)	)	PUNCT
eurjchem-267	71	45	.	.	PUNCT
eurjchem-267	72	1	the	the	DET
eurjchem-267	72	2	reaction	reaction	NOUN
eurjchem-267	72	3	mixture	mixture	NOUN
eurjchem-267	72	4	was	be	AUX
eurjchem-267	72	5	poured	pour	VERB
eurjchem-267	72	6	into	into	ADP
eurjchem-267	72	7	ice‐cooled	ice‐coole	VERB
eurjchem-267	72	8	water	water	NOUN
eurjchem-267	72	9	and	and	CCONJ
eurjchem-267	72	10	the	the	DET
eurjchem-267	72	11	solid	solid	ADJ
eurjchem-267	72	12	deposited	deposit	VERB
eurjchem-267	72	13	was	be	AUX
eurjchem-267	72	14	filtered	filter	VERB
eurjchem-267	72	15	off	off	ADP
eurjchem-267	72	16	,	,	PUNCT
eurjchem-267	72	17	dried	dry	VERB
eurjchem-267	72	18	and	and	CCONJ
eurjchem-267	72	19	then	then	ADV
eurjchem-267	72	20	recrystallized	recrystallize	VERB
eurjchem-267	72	21	from	from	ADP
eurjchem-267	72	22	ethanol	ethanol	NOUN
eurjchem-267	72	23	to	to	PART
eurjchem-267	72	24	give	give	VERB
eurjchem-267	72	25	4	4	NUM
eurjchem-267	72	26	as	as	ADP
eurjchem-267	72	27	pale	pale	ADJ
eurjchem-267	72	28	yellow	yellow	ADJ
eurjchem-267	72	29	crystals	crystal	NOUN
eurjchem-267	72	30	(	(	PUNCT
eurjchem-267	72	31	scheme	scheme	NOUN
eurjchem-267	72	32	1	1	NUM
eurjchem-267	72	33	and	and	CCONJ
eurjchem-267	72	34	2	2	NUM
eurjchem-267	72	35	)	)	PUNCT
eurjchem-267	72	36	.	.	PUNCT
eurjchem-267	73	1	yield	yield	NOUN
eurjchem-267	73	2	:	:	PUNCT
eurjchem-267	73	3	32.2	32.2	NUM
eurjchem-267	73	4	%	%	NOUN
eurjchem-267	73	5	.	.	PUNCT
eurjchem-267	74	1	m.p	m.p	PROPN
eurjchem-267	74	2	.	.	PROPN
eurjchem-267	74	3	:	:	PUNCT
eurjchem-267	75	1	202‐204	202‐204	NUM
eurjchem-267	75	2	oc	oc	NOUN
eurjchem-267	75	3	.	.	PUNCT
eurjchem-267	75	4	ft‐ir	ft‐ir	NOUN
eurjchem-267	75	5	(	(	PUNCT
eurjchem-267	75	6	kbr	kbr	PROPN
eurjchem-267	75	7	,	,	PUNCT
eurjchem-267	75	8	cm‐1	cm‐1	PROPN
eurjchem-267	75	9	):	):	PUNCT
eurjchem-267	75	10	3293	3293	NUM
eurjchem-267	75	11	ν(nh	ν(nh	NOUN
eurjchem-267	75	12	)	)	PUNCT
eurjchem-267	75	13	,	,	PUNCT
eurjchem-267	75	14	1711	1711	NUM
eurjchem-267	75	15	ν(c	ν(c	NOUN
eurjchem-267	75	16	=	=	SYM
eurjchem-267	75	17	o	o	NOUN
eurjchem-267	75	18	)	)	PUNCT
eurjchem-267	75	19	,	,	PUNCT
eurjchem-267	75	20	1652	1652	NUM
eurjchem-267	75	21	ν(c	ν(c	NOUN
eurjchem-267	75	22	=	=	SYM
eurjchem-267	75	23	oamide	oamide	ADV
eurjchem-267	75	24	)	)	PUNCT
eurjchem-267	75	25	,	,	PUNCT
eurjchem-267	75	26	1626	1626	NUM
eurjchem-267	75	27	ν(c	ν(c	NOUN
eurjchem-267	75	28	=	=	SYM
eurjchem-267	75	29	n	n	NUM
eurjchem-267	75	30	)	)	PUNCT
eurjchem-267	75	31	.	.	PUNCT
eurjchem-267	76	1	1h	1h	NUM
eurjchem-267	76	2	nmr	nmr	NOUN
eurjchem-267	76	3	(	(	PUNCT
eurjchem-267	76	4	200	200	NUM
eurjchem-267	76	5	mhz	mhz	NOUN
eurjchem-267	76	6	,	,	PUNCT
eurjchem-267	76	7	dmso‐d6	dmso‐d6	NUM
eurjchem-267	76	8	):	):	PUNCT
eurjchem-267	76	9	9.2	9.2	NUM
eurjchem-267	76	10	(	(	PUNCT
eurjchem-267	76	11	s	s	PROPN
eurjchem-267	76	12	,	,	PUNCT
eurjchem-267	76	13	1h	1h	NUM
eurjchem-267	76	14	,	,	PUNCT
eurjchem-267	76	15	exchangeable	exchangeable	ADJ
eurjchem-267	76	16	with	with	ADP
eurjchem-267	76	17	d2o	d2o	NOUN
eurjchem-267	76	18	)	)	PUNCT
eurjchem-267	76	19	,	,	PUNCT
eurjchem-267	76	20	8.3	8.3	NUM
eurjchem-267	76	21	(	(	PUNCT
eurjchem-267	76	22	s	s	PROPN
eurjchem-267	76	23	,	,	PUNCT
eurjchem-267	76	24	1h	1h	NUM
eurjchem-267	76	25	)	)	PUNCT
eurjchem-267	76	26	,	,	PUNCT
eurjchem-267	76	27	8.1‐6.9	8.1‐6.9	NUM
eurjchem-267	76	28	(	(	PUNCT
eurjchem-267	76	29	m	m	PROPN
eurjchem-267	76	30	,	,	PUNCT
eurjchem-267	76	31	18harom	18harom	NUM
eurjchem-267	76	32	.	.	PUNCT
eurjchem-267	76	33	)	)	PUNCT
eurjchem-267	76	34	,	,	PUNCT
eurjchem-267	76	35	6.36	6.36	NUM
eurjchem-267	76	36	(	(	PUNCT
eurjchem-267	76	37	m	m	PROPN
eurjchem-267	76	38	,	,	PUNCT
eurjchem-267	76	39	3h	3h	NUM
eurjchem-267	76	40	)	)	PUNCT
eurjchem-267	76	41	.	.	PUNCT
eurjchem-267	77	1	ms	ms	NOUN
eurjchem-267	77	2	(	(	PUNCT
eurjchem-267	77	3	ei	ei	PROPN
eurjchem-267	77	4	,	,	PUNCT
eurjchem-267	77	5	m	m	PROPN
eurjchem-267	77	6	/	/	SYM
eurjchem-267	77	7	z	z	PROPN
eurjchem-267	77	8	(	(	PUNCT
eurjchem-267	77	9	%	%	NOUN
eurjchem-267	77	10	)	)	PUNCT
eurjchem-267	77	11	):	):	PUNCT
eurjchem-267	77	12	533	533	NUM
eurjchem-267	77	13	(	(	PUNCT
eurjchem-267	77	14	m+2	m+2	NOUN
eurjchem-267	77	15	,	,	PUNCT
eurjchem-267	77	16	4.3	4.3	NUM
eurjchem-267	77	17	)	)	PUNCT
eurjchem-267	77	18	,	,	PUNCT
eurjchem-267	77	19	531	531	NUM
eurjchem-267	77	20	(	(	PUNCT
eurjchem-267	77	21	m+	m+	NUM
eurjchem-267	77	22	.	.	PROPN
eurjchem-267	77	23	,	,	PUNCT
eurjchem-267	77	24	12.7	12.7	NUM
eurjchem-267	77	25	)	)	PUNCT
eurjchem-267	77	26	,	,	PUNCT
eurjchem-267	77	27	393	393	NUM
eurjchem-267	77	28	(	(	PUNCT
eurjchem-267	77	29	32.3	32.3	NUM
eurjchem-267	77	30	)	)	PUNCT
eurjchem-267	77	31	,	,	PUNCT
eurjchem-267	77	32	146	146	NUM
eurjchem-267	77	33	(	(	PUNCT
eurjchem-267	77	34	100	100	NUM
eurjchem-267	77	35	)	)	PUNCT
eurjchem-267	77	36	,	,	PUNCT
eurjchem-267	77	37	105	105	NUM
eurjchem-267	77	38	(	(	PUNCT
eurjchem-267	77	39	92.8	92.8	NUM
eurjchem-267	77	40	)	)	PUNCT
eurjchem-267	77	41	,	,	PUNCT
eurjchem-267	77	42	77	77	NUM
eurjchem-267	77	43	(	(	PUNCT
eurjchem-267	77	44	62.4	62.4	NUM
eurjchem-267	77	45	)	)	PUNCT
eurjchem-267	77	46	.	.	PUNCT
eurjchem-267	78	1	anal	anal	PROPN
eurjchem-267	78	2	.	.	PUNCT
eurjchem-267	78	3	calcd	calcd	NOUN
eurjchem-267	78	4	.	.	PUNCT
eurjchem-267	79	1	for	for	ADP
eurjchem-267	79	2	c32h23cln4o2	c32h23cln4o2	PROPN
eurjchem-267	79	3	(	(	PUNCT
eurjchem-267	79	4	530.5	530.5	NUM
eurjchem-267	79	5	):	):	PUNCT
eurjchem-267	79	6	c	c	NOUN
eurjchem-267	79	7	,	,	PUNCT
eurjchem-267	79	8	72.38;	72.38;	NUM
eurjchem-267	79	9	h	h	NOUN
eurjchem-267	79	10	,	,	PUNCT
eurjchem-267	79	11	4.33	4.33	NUM
eurjchem-267	79	12	;	;	PUNCT
eurjchem-267	79	13	n	n	CCONJ
eurjchem-267	79	14	,	,	PUNCT
eurjchem-267	79	15	10.55	10.55	NUM
eurjchem-267	79	16	;	;	PUNCT
eurjchem-267	79	17	cl	cl	NOUN
eurjchem-267	79	18	,	,	PUNCT
eurjchem-267	79	19	6.69	6.69	NUM
eurjchem-267	79	20	.	.	PUNCT
eurjchem-267	79	21	found	find	VERB
eurjchem-267	79	22	:	:	PUNCT
eurjchem-267	80	1	c	c	X
eurjchem-267	80	2	,	,	PUNCT
eurjchem-267	80	3	72.48	72.48	NUM
eurjchem-267	80	4	;	;	PUNCT
eurjchem-267	80	5	h	h	NOUN
eurjchem-267	80	6	,	,	PUNCT
eurjchem-267	80	7	4.13	4.13	NUM
eurjchem-267	80	8	;	;	PUNCT
eurjchem-267	80	9	n	n	CCONJ
eurjchem-267	80	10	,	,	PUNCT
eurjchem-267	80	11	10.45	10.45	NUM
eurjchem-267	80	12	;	;	PUNCT
eurjchem-267	80	13	cl	cl	NOUN
eurjchem-267	80	14	,	,	PUNCT
eurjchem-267	80	15	6.83	6.83	NUM
eurjchem-267	80	16	%	%	NOUN
eurjchem-267	80	17	.	.	PUNCT
eurjchem-267	81	1	2.5	2.5	NUM
eurjchem-267	81	2	.	.	PUNCT
eurjchem-267	82	1	2‐[n‐(2z,4e)‐1‐benzamido‐1‐oxo‐5‐phenylpenta‐2,4‐	2‐[n‐(2z,4e)‐1‐benzamido‐1‐oxo‐5‐phenylpenta‐2,4‐	NUM
eurjchem-267	82	2	dien‐2‐yl]amino	dien‐2‐yl]amino	PROPN
eurjchem-267	82	3	benzoic	benzoic	ADJ
eurjchem-267	82	4	acid	acid	NOUN
eurjchem-267	82	5	hydrazide	hydrazide	ADV
eurjchem-267	82	6	(	(	PUNCT
eurjchem-267	82	7	5	5	NUM
eurjchem-267	82	8	)	)	PUNCT
eurjchem-267	82	9	to	to	ADP
eurjchem-267	82	10	a	a	DET
eurjchem-267	82	11	solution	solution	NOUN
eurjchem-267	82	12	of	of	ADP
eurjchem-267	82	13	1	1	NUM
eurjchem-267	82	14	(	(	PUNCT
eurjchem-267	82	15	1.2	1.2	NUM
eurjchem-267	82	16	g	g	NOUN
eurjchem-267	82	17	,	,	PUNCT
eurjchem-267	82	18	0.003	0.003	NUM
eurjchem-267	82	19	mole	mole	NOUN
eurjchem-267	82	20	)	)	PUNCT
eurjchem-267	82	21	in	in	ADP
eurjchem-267	82	22	absolute	absolute	ADJ
eurjchem-267	82	23	ethanol	ethanol	NOUN
eurjchem-267	82	24	(	(	PUNCT
eurjchem-267	82	25	30	30	NUM
eurjchem-267	82	26	ml	ml	NOUN
eurjchem-267	82	27	)	)	PUNCT
eurjchem-267	82	28	,	,	PUNCT
eurjchem-267	82	29	hydrazine	hydrazine	NOUN
eurjchem-267	82	30	hydrate	hydrate	NOUN
eurjchem-267	82	31	(	(	PUNCT
eurjchem-267	82	32	0.003	0.003	NUM
eurjchem-267	82	33	mol	mol	NOUN
eurjchem-267	82	34	,	,	PUNCT
eurjchem-267	82	35	80	80	NUM
eurjchem-267	82	36	%	%	NOUN
eurjchem-267	82	37	)	)	PUNCT
eurjchem-267	82	38	was	be	AUX
eurjchem-267	82	39	added	add	VERB
eurjchem-267	82	40	dropwise	dropwise	NOUN
eurjchem-267	82	41	with	with	ADP
eurjchem-267	82	42	stirring	stir	VERB
eurjchem-267	82	43	at	at	ADP
eurjchem-267	82	44	room	room	NOUN
eurjchem-267	82	45	temperature	temperature	NOUN
eurjchem-267	82	46	for	for	ADP
eurjchem-267	82	47	2	2	NUM
eurjchem-267	82	48	hrs	hrs	NOUN
eurjchem-267	82	49	(	(	PUNCT
eurjchem-267	82	50	tlc	tlc	NOUN
eurjchem-267	82	51	)	)	PUNCT
eurjchem-267	82	52	.	.	PUNCT
eurjchem-267	83	1	the	the	DET
eurjchem-267	83	2	separated	separate	VERB
eurjchem-267	83	3	solid	solid	ADJ
eurjchem-267	83	4	was	be	AUX
eurjchem-267	83	5	filtered	filter	VERB
eurjchem-267	83	6	off	off	ADP
eurjchem-267	83	7	,	,	PUNCT
eurjchem-267	83	8	dried	dry	VERB
eurjchem-267	83	9	and	and	CCONJ
eurjchem-267	83	10	recrystallized	recrystallize	VERB
eurjchem-267	83	11	from	from	ADP
eurjchem-267	83	12	benzene	benzene	NOUN
eurjchem-267	83	13	to	to	PART
eurjchem-267	83	14	give	give	VERB
eurjchem-267	83	15	5	5	NUM
eurjchem-267	83	16	as	as	ADP
eurjchem-267	83	17	colourless	colourless	ADJ
eurjchem-267	83	18	crystals	crystal	NOUN
eurjchem-267	83	19	(	(	PUNCT
eurjchem-267	83	20	scheme	scheme	NOUN
eurjchem-267	83	21	3	3	NUM
eurjchem-267	83	22	)	)	PUNCT
eurjchem-267	83	23	.	.	PUNCT
eurjchem-267	84	1	yield	yield	NOUN
eurjchem-267	84	2	:	:	PUNCT
eurjchem-267	84	3	81.3	81.3	NUM
eurjchem-267	84	4	%	%	NOUN
eurjchem-267	84	5	.	.	PUNCT
eurjchem-267	85	1	m.p	m.p	PROPN
eurjchem-267	85	2	.	.	PROPN
eurjchem-267	85	3	:	:	PUNCT
eurjchem-267	86	1	132‐134	132‐134	NUM
eurjchem-267	86	2	oc	oc	NOUN
eurjchem-267	86	3	.	.	PUNCT
eurjchem-267	86	4	ft‐ir	ft‐ir	NOUN
eurjchem-267	86	5	(	(	PUNCT
eurjchem-267	86	6	kbr	kbr	PROPN
eurjchem-267	86	7	,	,	PUNCT
eurjchem-267	86	8	cm‐1	cm‐1	PROPN
eurjchem-267	86	9	):	):	PUNCT
eurjchem-267	86	10	3540	3540	NUM
eurjchem-267	86	11	,	,	PUNCT
eurjchem-267	86	12	3331	3331	NUM
eurjchem-267	86	13	,	,	PUNCT
eurjchem-267	86	14	3232	3232	NUM
eurjchem-267	86	15	ν(nh2	ν(nh2	PROPN
eurjchem-267	86	16	,	,	PUNCT
eurjchem-267	86	17	nh	nh	PROPN
eurjchem-267	86	18	)	)	PUNCT
eurjchem-267	86	19	,	,	PUNCT
eurjchem-267	86	20	1683	1683	NUM
eurjchem-267	86	21	ν(c	ν(c	PROPN
eurjchem-267	86	22	=	=	SYM
eurjchem-267	86	23	o	o	NOUN
eurjchem-267	86	24	)	)	PUNCT
eurjchem-267	86	25	,	,	PUNCT
eurjchem-267	86	26	1650	1650	NUM
eurjchem-267	86	27	ν(c	ν(c	PROPN
eurjchem-267	86	28	=	=	SYM
eurjchem-267	86	29	o	o	NOUN
eurjchem-267	86	30	)	)	PUNCT
eurjchem-267	86	31	.	.	PUNCT
eurjchem-267	87	1	1h	1h	NUM
eurjchem-267	87	2	nmr	nmr	NOUN
eurjchem-267	87	3	(	(	PUNCT
eurjchem-267	87	4	200	200	NUM
eurjchem-267	87	5	mhz	mhz	NOUN
eurjchem-267	87	6	,	,	PUNCT
eurjchem-267	87	7	cdcl3	cdcl3	NOUN
eurjchem-267	87	8	):	):	PUNCT
eurjchem-267	87	9	9.3	9.3	NUM
eurjchem-267	87	10	(	(	PUNCT
eurjchem-267	87	11	br.s	br.s	PROPN
eurjchem-267	87	12	,	,	PUNCT
eurjchem-267	87	13	1h	1h	NUM
eurjchem-267	87	14	,	,	PUNCT
eurjchem-267	87	15	exchangeable	exchangeable	ADJ
eurjchem-267	87	16	with	with	ADP
eurjchem-267	87	17	d2o	d2o	NOUN
eurjchem-267	87	18	)	)	PUNCT
eurjchem-267	87	19	,	,	PUNCT
eurjchem-267	87	20	9.0	9.0	NUM
eurjchem-267	87	21	(	(	PUNCT
eurjchem-267	87	22	br.s	br.s	PROPN
eurjchem-267	87	23	,	,	PUNCT
eurjchem-267	87	24	2h	2h	NUM
eurjchem-267	87	25	,	,	PUNCT
eurjchem-267	87	26	exchangeable	exchangeable	ADJ
eurjchem-267	87	27	with	with	ADP
eurjchem-267	87	28	d2o	d2o	NOUN
eurjchem-267	87	29	)	)	PUNCT
eurjchem-267	87	30	,	,	PUNCT
eurjchem-267	87	31	8.04‐7.20	8.04‐7.20	NUM
eurjchem-267	87	32	(	(	PUNCT
eurjchem-267	87	33	m	m	PROPN
eurjchem-267	87	34	,	,	PUNCT
eurjchem-267	87	35	14harom	14harom	NUM
eurjchem-267	87	36	.	.	PUNCT
eurjchem-267	87	37	)	)	PUNCT
eurjchem-267	87	38	,	,	PUNCT
eurjchem-267	87	39	6.9	6.9	NUM
eurjchem-267	87	40	(	(	PUNCT
eurjchem-267	87	41	br.s	br.s	PROPN
eurjchem-267	87	42	,	,	PUNCT
eurjchem-267	87	43	3h	3h	NUM
eurjchem-267	87	44	)	)	PUNCT
eurjchem-267	87	45	,	,	PUNCT
eurjchem-267	87	46	4.2	4.2	NUM
eurjchem-267	87	47	(	(	PUNCT
eurjchem-267	87	48	br.s	br.s	PROPN
eurjchem-267	87	49	,	,	PUNCT
eurjchem-267	87	50	2h	2h	NUM
eurjchem-267	87	51	,	,	PUNCT
eurjchem-267	87	52	exchangeable	exchangeable	ADJ
eurjchem-267	87	53	with	with	ADP
eurjchem-267	87	54	d2o	d2o	NOUN
eurjchem-267	87	55	)	)	PUNCT
eurjchem-267	87	56	.	.	PUNCT
eurjchem-267	88	1	ms	ms	NOUN
eurjchem-267	88	2	(	(	PUNCT
eurjchem-267	88	3	ei	ei	PROPN
eurjchem-267	88	4	,	,	PUNCT
eurjchem-267	88	5	m	m	PROPN
eurjchem-267	88	6	/	/	SYM
eurjchem-267	88	7	z	z	PROPN
eurjchem-267	88	8	(	(	PUNCT
eurjchem-267	88	9	%	%	NOUN
eurjchem-267	88	10	)	)	PUNCT
eurjchem-267	88	11	):	):	PUNCT
eurjchem-267	88	12	426	426	NUM
eurjchem-267	88	13	(	(	PUNCT
eurjchem-267	88	14	m+	m+	NUM
eurjchem-267	88	15	.	.	PROPN
eurjchem-267	88	16	,	,	PUNCT
eurjchem-267	88	17	23.6	23.6	NUM
eurjchem-267	88	18	)	)	PUNCT
eurjchem-267	88	19	,	,	PUNCT
eurjchem-267	88	20	395	395	NUM
eurjchem-267	88	21	(	(	PUNCT
eurjchem-267	88	22	33.1	33.1	NUM
eurjchem-267	88	23	)	)	PUNCT
eurjchem-267	88	24	,	,	PUNCT
eurjchem-267	88	25	367	367	NUM
eurjchem-267	88	26	(	(	PUNCT
eurjchem-267	88	27	60.4	60.4	NUM
eurjchem-267	88	28	)	)	PUNCT
eurjchem-267	88	29	,	,	PUNCT
eurjchem-267	88	30	178	178	NUM
eurjchem-267	88	31	(	(	PUNCT
eurjchem-267	88	32	100	100	NUM
eurjchem-267	88	33	)	)	PUNCT
eurjchem-267	88	34	,	,	PUNCT
eurjchem-267	88	35	105	105	NUM
eurjchem-267	88	36	(	(	PUNCT
eurjchem-267	88	37	90.2	90.2	NUM
eurjchem-267	88	38	)	)	PUNCT
eurjchem-267	88	39	,	,	PUNCT
eurjchem-267	88	40	77	77	NUM
eurjchem-267	88	41	(	(	PUNCT
eurjchem-267	88	42	66.1	66.1	NUM
eurjchem-267	88	43	)	)	PUNCT
eurjchem-267	88	44	.	.	PUNCT
eurjchem-267	89	1	anal	anal	PROPN
eurjchem-267	89	2	.	.	PUNCT
eurjchem-267	89	3	calcd	calcd	NOUN
eurjchem-267	89	4	.	.	PUNCT
eurjchem-267	90	1	for	for	ADP
eurjchem-267	90	2	c25h22n4o3	c25h22n4o3	PROPN
eurjchem-267	90	3	(	(	PUNCT
eurjchem-267	90	4	426	426	NUM
eurjchem-267	90	5	):	):	PUNCT
eurjchem-267	90	6	c	c	X
eurjchem-267	90	7	,	,	PUNCT
eurjchem-267	90	8	70.42;	70.42;	NUM
eurjchem-267	90	9	h	h	NOUN
eurjchem-267	90	10	,	,	PUNCT
eurjchem-267	90	11	5.16	5.16	NUM
eurjchem-267	90	12	;	;	PUNCT
eurjchem-267	90	13	n	n	CCONJ
eurjchem-267	90	14	,	,	PUNCT
eurjchem-267	90	15	13.14	13.14	NUM
eurjchem-267	90	16	.	.	PUNCT
eurjchem-267	91	1	found	find	VERB
eurjchem-267	91	2	:	:	PUNCT
eurjchem-267	92	1	c	c	X
eurjchem-267	92	2	,	,	PUNCT
eurjchem-267	92	3	70.42	70.42	NUM
eurjchem-267	92	4	;	;	PUNCT
eurjchem-267	92	5	h	h	NOUN
eurjchem-267	92	6	,	,	PUNCT
eurjchem-267	92	7	5.40	5.40	NUM
eurjchem-267	92	8	;	;	PUNCT
eurjchem-267	92	9	n	n	CCONJ
eurjchem-267	92	10	,	,	PUNCT
eurjchem-267	92	11	13.09	13.09	NUM
eurjchem-267	92	12	%	%	NOUN
eurjchem-267	92	13	.	.	PUNCT
eurjchem-267	93	1	2.6	2.6	NUM
eurjchem-267	93	2	.	.	PUNCT
eurjchem-267	94	1	3‐amino‐2‐[(1z,3e)‐1‐benzamido‐4‐phenyl‐1,3‐buta‐	3‐amino‐2‐[(1z,3e)‐1‐benzamido‐4‐phenyl‐1,3‐buta‐	PROPN
eurjchem-267	94	2	dien‐1‐yl]quinazolin‐4(h)‐one(6	dien‐1‐yl]quinazolin‐4(h)‐one(6	PROPN
eurjchem-267	94	3	)	)	PUNCT
eurjchem-267	94	4	a	a	DET
eurjchem-267	94	5	mixture	mixture	NOUN
eurjchem-267	94	6	of	of	ADP
eurjchem-267	94	7	1	1	NUM
eurjchem-267	94	8	(	(	PUNCT
eurjchem-267	94	9	0.01	0.01	NUM
eurjchem-267	94	10	mol	mol	NOUN
eurjchem-267	94	11	)	)	PUNCT
eurjchem-267	94	12	,	,	PUNCT
eurjchem-267	94	13	hydrazine	hydrazine	NOUN
eurjchem-267	94	14	hydrate	hydrate	NOUN
eurjchem-267	94	15	(	(	PUNCT
eurjchem-267	94	16	0.03	0.03	NUM
eurjchem-267	94	17	mol	mol	NOUN
eurjchem-267	94	18	,	,	PUNCT
eurjchem-267	94	19	80	80	NUM
eurjchem-267	94	20	%	%	NOUN
eurjchem-267	94	21	)	)	PUNCT
eurjchem-267	94	22	in	in	ADP
eurjchem-267	94	23	absolute	absolute	ADJ
eurjchem-267	94	24	ethanol	ethanol	NOUN
eurjchem-267	94	25	(	(	PUNCT
eurjchem-267	94	26	30	30	NUM
eurjchem-267	94	27	ml	ml	NOUN
eurjchem-267	94	28	)	)	PUNCT
eurjchem-267	94	29	was	be	AUX
eurjchem-267	94	30	refluxed	refluxe	VERB
eurjchem-267	94	31	for	for	ADP
eurjchem-267	94	32	10	10	NUM
eurjchem-267	94	33	hrs	hrs	NOUN
eurjchem-267	94	34	(	(	PUNCT
eurjchem-267	94	35	tlc	tlc	NOUN
eurjchem-267	94	36	)	)	PUNCT
eurjchem-267	94	37	.	.	PUNCT
eurjchem-267	95	1	evaporation	evaporation	NOUN
eurjchem-267	95	2	of	of	ADP
eurjchem-267	95	3	excess	excess	ADJ
eurjchem-267	95	4	ethanol	ethanol	NOUN
eurjchem-267	95	5	left	leave	VERB
eurjchem-267	95	6	a	a	DET
eurjchem-267	95	7	crude	crude	ADJ
eurjchem-267	95	8	product	product	NOUN
eurjchem-267	95	9	which	which	PRON
eurjchem-267	95	10	filtered	filter	VERB
eurjchem-267	95	11	off	off	ADP
eurjchem-267	95	12	,	,	PUNCT
eurjchem-267	95	13	dried	dry	VERB
eurjchem-267	95	14	and	and	CCONJ
eurjchem-267	95	15	recrystallized	recrystallize	VERB
eurjchem-267	95	16	from	from	ADP
eurjchem-267	95	17	toluene	toluene	NOUN
eurjchem-267	95	18	to	to	PART
eurjchem-267	95	19	give	give	VERB
eurjchem-267	95	20	6	6	NUM
eurjchem-267	95	21	as	as	ADP
eurjchem-267	95	22	pale	pale	ADJ
eurjchem-267	95	23	yellow	yellow	ADJ
eurjchem-267	95	24	crystals	crystal	NOUN
eurjchem-267	95	25	(	(	PUNCT
eurjchem-267	95	26	scheme	scheme	NOUN
eurjchem-267	95	27	1	1	NUM
eurjchem-267	95	28	and	and	CCONJ
eurjchem-267	95	29	2	2	NUM
eurjchem-267	95	30	)	)	PUNCT
eurjchem-267	95	31	.	.	PUNCT
eurjchem-267	96	1	yield	yield	NOUN
eurjchem-267	96	2	:	:	PUNCT
eurjchem-267	96	3	61.2	61.2	NUM
eurjchem-267	96	4	%	%	NOUN
eurjchem-267	96	5	.	.	PUNCT
eurjchem-267	97	1	m.p	m.p	PROPN
eurjchem-267	97	2	.	.	PROPN
eurjchem-267	97	3	:	:	PUNCT
eurjchem-267	98	1	174‐	174‐	NUM
eurjchem-267	98	2	176	176	NUM
eurjchem-267	98	3	oc	oc	NOUN
eurjchem-267	98	4	.	.	PUNCT
eurjchem-267	99	1	ft‐ir	ft‐ir	NOUN
eurjchem-267	99	2	(	(	PUNCT
eurjchem-267	99	3	kbr	kbr	PROPN
eurjchem-267	99	4	,	,	PUNCT
eurjchem-267	99	5	cm‐1	cm‐1	PROPN
eurjchem-267	99	6	):	):	PUNCT
eurjchem-267	99	7	3392	3392	NUM
eurjchem-267	99	8	,	,	PUNCT
eurjchem-267	99	9	3273	3273	NUM
eurjchem-267	99	10	,	,	PUNCT
eurjchem-267	99	11	3172	3172	NUM
eurjchem-267	99	12	ν(nh2	ν(nh2	PROPN
eurjchem-267	99	13	)	)	PUNCT
eurjchem-267	99	14	,	,	PUNCT
eurjchem-267	99	15	1705	1705	NUM
eurjchem-267	99	16	,	,	PUNCT
eurjchem-267	99	17	1662	1662	NUM
eurjchem-267	99	18	ν(c	ν(c	PROPN
eurjchem-267	99	19	=	=	SYM
eurjchem-267	99	20	o	o	NOUN
eurjchem-267	99	21	)	)	PUNCT
eurjchem-267	99	22	,	,	PUNCT
eurjchem-267	99	23	1621	1621	NUM
eurjchem-267	99	24	ν(c	ν(c	PROPN
eurjchem-267	99	25	=	=	SYM
eurjchem-267	99	26	c	c	NOUN
eurjchem-267	99	27	)	)	PUNCT
eurjchem-267	99	28	.	.	PUNCT
eurjchem-267	100	1	1h	1h	NUM
eurjchem-267	100	2	nmr	nmr	NOUN
eurjchem-267	100	3	(	(	PUNCT
eurjchem-267	100	4	200	200	NUM
eurjchem-267	100	5	mhz	mhz	NOUN
eurjchem-267	100	6	,	,	PUNCT
eurjchem-267	100	7	cdcl3	cdcl3	NOUN
eurjchem-267	100	8	):	):	PUNCT
eurjchem-267	100	9	9.1	9.1	NUM
eurjchem-267	100	10	(	(	PUNCT
eurjchem-267	100	11	br.s	br.s	PROPN
eurjchem-267	100	12	,	,	PUNCT
eurjchem-267	100	13	1h	1h	NUM
eurjchem-267	100	14	,	,	PUNCT
eurjchem-267	100	15	exchangeable	exchangeable	ADJ
eurjchem-267	100	16	with	with	ADP
eurjchem-267	100	17	d2o	d2o	NOUN
eurjchem-267	100	18	)	)	PUNCT
eurjchem-267	100	19	,	,	PUNCT
eurjchem-267	100	20	8.7	8.7	NUM
eurjchem-267	100	21	(	(	PUNCT
eurjchem-267	100	22	br.s	br.s	PROPN
eurjchem-267	100	23	,	,	PUNCT
eurjchem-267	100	24	2h	2h	NUM
eurjchem-267	100	25	,	,	PUNCT
eurjchem-267	100	26	exchangeable	exchangeable	ADJ
eurjchem-267	100	27	with	with	ADP
eurjchem-267	100	28	d2o	d2o	NOUN
eurjchem-267	100	29	)	)	PUNCT
eurjchem-267	100	30	,	,	PUNCT
eurjchem-267	100	31	8.04‐7.20	8.04‐7.20	NUM
eurjchem-267	100	32	(	(	PUNCT
eurjchem-267	100	33	m	m	PROPN
eurjchem-267	100	34	,	,	PUNCT
eurjchem-267	100	35	14harom	14harom	NUM
eurjchem-267	100	36	.	.	PUNCT
eurjchem-267	100	37	)	)	PUNCT
eurjchem-267	100	38	,	,	PUNCT
eurjchem-267	100	39	6.8	6.8	NUM
eurjchem-267	100	40	(	(	PUNCT
eurjchem-267	100	41	br.s	br.s	PROPN
eurjchem-267	100	42	,	,	PUNCT
eurjchem-267	100	43	3h	3h	NUM
eurjchem-267	100	44	)	)	PUNCT
eurjchem-267	100	45	.	.	PUNCT
eurjchem-267	101	1	ms	ms	NOUN
eurjchem-267	101	2	(	(	PUNCT
eurjchem-267	101	3	ei	ei	PROPN
eurjchem-267	101	4	,	,	PUNCT
eurjchem-267	101	5	m	m	PROPN
eurjchem-267	101	6	/	/	SYM
eurjchem-267	101	7	z	z	PROPN
eurjchem-267	101	8	(	(	PUNCT
eurjchem-267	101	9	%	%	NOUN
eurjchem-267	101	10	)	)	PUNCT
eurjchem-267	101	11	):	):	PUNCT
eurjchem-267	101	12	408	408	NUM
eurjchem-267	101	13	(	(	PUNCT
eurjchem-267	101	14	m+	m+	NUM
eurjchem-267	101	15	.	.	PROPN
eurjchem-267	101	16	,	,	PUNCT
eurjchem-267	101	17	40.2	40.2	NUM
eurjchem-267	101	18	)	)	PUNCT
eurjchem-267	101	19	,	,	PUNCT
eurjchem-267	101	20	393	393	NUM
eurjchem-267	101	21	(	(	PUNCT
eurjchem-267	101	22	70.6	70.6	NUM
eurjchem-267	101	23	)	)	PUNCT
eurjchem-267	101	24	,	,	PUNCT
eurjchem-267	101	25	145	145	NUM
eurjchem-267	101	26	(	(	PUNCT
eurjchem-267	101	27	100	100	NUM
eurjchem-267	101	28	)	)	PUNCT
eurjchem-267	101	29	,	,	PUNCT
eurjchem-267	101	30	105	105	NUM
eurjchem-267	101	31	(	(	PUNCT
eurjchem-267	101	32	90.6	90.6	NUM
eurjchem-267	101	33	)	)	PUNCT
eurjchem-267	101	34	,	,	PUNCT
eurjchem-267	101	35	77	77	NUM
eurjchem-267	101	36	(	(	PUNCT
eurjchem-267	101	37	70.3	70.3	NUM
eurjchem-267	101	38	)	)	PUNCT
eurjchem-267	101	39	.	.	PUNCT
eurjchem-267	102	1	anal	anal	PROPN
eurjchem-267	102	2	.	.	PUNCT
eurjchem-267	102	3	calcd	calcd	NOUN
eurjchem-267	102	4	.	.	PUNCT
eurjchem-267	103	1	for	for	ADP
eurjchem-267	103	2	c25h20n4o2	c25h20n4o2	PROPN
eurjchem-267	103	3	(	(	PUNCT
eurjchem-267	103	4	408	408	NUM
eurjchem-267	103	5	):	):	PUNCT
eurjchem-267	103	6	c	c	NOUN
eurjchem-267	103	7	,	,	PUNCT
eurjchem-267	103	8	73.52;	73.52;	NUM
eurjchem-267	103	9	h	h	NOUN
eurjchem-267	103	10	,	,	PUNCT
eurjchem-267	103	11	4.9	4.9	NUM
eurjchem-267	103	12	;	;	PUNCT
eurjchem-267	103	13	n	n	CCONJ
eurjchem-267	103	14	,	,	PUNCT
eurjchem-267	103	15	13.72	13.72	NUM
eurjchem-267	103	16	.	.	PUNCT
eurjchem-267	103	17	found	find	VERB
eurjchem-267	103	18	:	:	PUNCT
eurjchem-267	104	1	c	c	X
eurjchem-267	104	2	,	,	PUNCT
eurjchem-267	104	3	73.38	73.38	NUM
eurjchem-267	104	4	;	;	PUNCT
eurjchem-267	104	5	h	h	NOUN
eurjchem-267	104	6	,	,	PUNCT
eurjchem-267	104	7	5.02	5.02	NUM
eurjchem-267	104	8	;	;	PUNCT
eurjchem-267	104	9	n	n	CCONJ
eurjchem-267	104	10	,	,	PUNCT
eurjchem-267	104	11	13.83	13.83	NUM
eurjchem-267	104	12	%	%	NOUN
eurjchem-267	104	13	.	.	PUNCT
eurjchem-267	105	1	2.7	2.7	NUM
eurjchem-267	105	2	.	.	PUNCT
eurjchem-267	106	1	reaction	reaction	NOUN
eurjchem-267	106	2	of	of	ADP
eurjchem-267	106	3	6	6	NUM
eurjchem-267	106	4	with	with	ADP
eurjchem-267	106	5	aromatic	aromatic	ADJ
eurjchem-267	106	6	aldehydes	aldehyde	NOUN
eurjchem-267	106	7	compound	compound	VERB
eurjchem-267	106	8	6	6	NUM
eurjchem-267	106	9	(	(	PUNCT
eurjchem-267	106	10	1.2	1.2	NUM
eurjchem-267	106	11	g	g	NOUN
eurjchem-267	106	12	,	,	PUNCT
eurjchem-267	106	13	0.003	0.003	NUM
eurjchem-267	106	14	mol	mol	NOUN
eurjchem-267	106	15	)	)	PUNCT
eurjchem-267	106	16	was	be	AUX
eurjchem-267	106	17	dissolved	dissolve	VERB
eurjchem-267	106	18	in	in	ADP
eurjchem-267	106	19	absolute	absolute	ADJ
eurjchem-267	106	20	ethanol	ethanol	NOUN
eurjchem-267	106	21	(	(	PUNCT
eurjchem-267	106	22	30	30	NUM
eurjchem-267	106	23	ml	ml	NOUN
eurjchem-267	106	24	)	)	PUNCT
eurjchem-267	106	25	and	and	CCONJ
eurjchem-267	106	26	p‐chlorobenzaldehyde	p‐chlorobenzaldehyde	NUM
eurjchem-267	106	27	(	(	PUNCT
eurjchem-267	106	28	0.42	0.42	NUM
eurjchem-267	106	29	g	g	NOUN
eurjchem-267	106	30	,	,	PUNCT
eurjchem-267	106	31	0.003	0.003	NUM
eurjchem-267	106	32	mol	mol	NOUN
eurjchem-267	106	33	)	)	PUNCT
eurjchem-267	106	34	was	be	AUX
eurjchem-267	106	35	added	add	VERB
eurjchem-267	106	36	dropwise	dropwise	NOUN
eurjchem-267	106	37	with	with	ADP
eurjchem-267	106	38	stirring	stir	VERB
eurjchem-267	106	39	at	at	ADP
eurjchem-267	106	40	room	room	NOUN
eurjchem-267	106	41	temperature	temperature	NOUN
eurjchem-267	106	42	for	for	ADP
eurjchem-267	106	43	30	30	NUM
eurjchem-267	106	44	min	min	NOUN
eurjchem-267	106	45	.	.	PROPN
eurjchem-267	106	46	,	,	PUNCT
eurjchem-267	106	47	then	then	ADV
eurjchem-267	106	48	the	the	DET
eurjchem-267	106	49	reaction	reaction	NOUN
eurjchem-267	106	50	mixture	mixture	NOUN
eurjchem-267	106	51	was	be	AUX
eurjchem-267	106	52	refluxed	refluxe	VERB
eurjchem-267	106	53	for	for	ADP
eurjchem-267	106	54	3	3	NUM
eurjchem-267	106	55	hrs	hrs	NOUN
eurjchem-267	106	56	(	(	PUNCT
eurjchem-267	106	57	tlc	tlc	NOUN
eurjchem-267	106	58	)	)	PUNCT
eurjchem-267	106	59	.	.	PUNCT
eurjchem-267	107	1	evaporation	evaporation	NOUN
eurjchem-267	107	2	of	of	ADP
eurjchem-267	107	3	the	the	DET
eurjchem-267	107	4	solvent	solvent	NOUN
eurjchem-267	107	5	left	leave	VERB
eurjchem-267	107	6	a	a	DET
eurjchem-267	107	7	crude	crude	ADJ
eurjchem-267	107	8	product	product	NOUN
eurjchem-267	107	9	which	which	PRON
eurjchem-267	107	10	filtered	filter	VERB
eurjchem-267	107	11	off	off	ADP
eurjchem-267	107	12	,	,	PUNCT
eurjchem-267	107	13	dried	dry	VERB
eurjchem-267	107	14	and	and	CCONJ
eurjchem-267	107	15	recrystallized	recrystallize	VERB
eurjchem-267	107	16	from	from	ADP
eurjchem-267	107	17	ethanol	ethanol	NOUN
eurjchem-267	107	18	to	to	PART
eurjchem-267	107	19	give	give	VERB
eurjchem-267	107	20	4	4	NUM
eurjchem-267	107	21	(	(	PUNCT
eurjchem-267	107	22	identity	identity	NOUN
eurjchem-267	107	23	m.p	m.p	PROPN
eurjchem-267	107	24	,	,	PUNCT
eurjchem-267	107	25	mixed	mixed	ADJ
eurjchem-267	107	26	m.p	m.p	PROPN
eurjchem-267	107	27	,	,	PUNCT
eurjchem-267	107	28	tlc	tlc	NOUN
eurjchem-267	107	29	,	,	PUNCT
eurjchem-267	107	30	ir	ir	PROPN
eurjchem-267	107	31	)	)	PUNCT
eurjchem-267	107	32	.	.	PUNCT
eurjchem-267	108	1	2.8	2.8	NUM
eurjchem-267	108	2	.	.	PUNCT
eurjchem-267	108	3	1,2,3‐triazino[6,1‐b]quinazolin‐10(4h)‐one	1,2,3‐triazino[6,1‐b]quinazolin‐10(4h)‐one	NUM
eurjchem-267	108	4	(	(	PUNCT
eurjchem-267	108	5	7	7	NUM
eurjchem-267	108	6	)	)	PUNCT
eurjchem-267	108	7	to	to	ADP
eurjchem-267	108	8	a	a	DET
eurjchem-267	108	9	stirred	stir	VERB
eurjchem-267	108	10	solution	solution	NOUN
eurjchem-267	108	11	of	of	ADP
eurjchem-267	108	12	1	1	NUM
eurjchem-267	108	13	(	(	PUNCT
eurjchem-267	108	14	0.01	0.01	NUM
eurjchem-267	108	15	mol	mol	NOUN
eurjchem-267	108	16	)	)	PUNCT
eurjchem-267	108	17	in	in	ADP
eurjchem-267	108	18	n‐butanol	n‐butanol	PROPN
eurjchem-267	108	19	(	(	PUNCT
eurjchem-267	108	20	20	20	NUM
eurjchem-267	108	21	ml	ml	NOUN
eurjchem-267	108	22	)	)	PUNCT
eurjchem-267	108	23	,	,	PUNCT
eurjchem-267	108	24	hydrazine	hydrazine	NOUN
eurjchem-267	108	25	hydrate	hydrate	NOUN
eurjchem-267	108	26	(	(	PUNCT
eurjchem-267	108	27	0.03	0.03	NUM
eurjchem-267	108	28	mol	mol	NOUN
eurjchem-267	108	29	,	,	PUNCT
eurjchem-267	108	30	80	80	NUM
eurjchem-267	108	31	%	%	NOUN
eurjchem-267	108	32	)	)	PUNCT
eurjchem-267	108	33	was	be	AUX
eurjchem-267	108	34	added	add	VERB
eurjchem-267	108	35	and	and	CCONJ
eurjchem-267	108	36	the	the	DET
eurjchem-267	108	37	reaction	reaction	NOUN
eurjchem-267	108	38	mixture	mixture	NOUN
eurjchem-267	108	39	was	be	AUX
eurjchem-267	108	40	refluxed	refluxe	VERB
eurjchem-267	108	41	for	for	ADP
eurjchem-267	108	42	16	16	NUM
eurjchem-267	108	43	hrs	hrs	NOUN
eurjchem-267	108	44	(	(	PUNCT
eurjchem-267	108	45	tlc	tlc	NOUN
eurjchem-267	108	46	)	)	PUNCT
eurjchem-267	108	47	.	.	PUNCT
eurjchem-267	109	1	the	the	DET
eurjchem-267	109	2	excess	excess	ADJ
eurjchem-267	109	3	solvent	solvent	NOUN
eurjchem-267	109	4	was	be	AUX
eurjchem-267	109	5	evaporated	evaporate	VERB
eurjchem-267	109	6	under	under	ADP
eurjchem-267	109	7	reduced	reduced	ADJ
eurjchem-267	109	8	pressure	pressure	NOUN
eurjchem-267	109	9	.	.	PUNCT
eurjchem-267	110	1	the	the	DET
eurjchem-267	110	2	residual	residual	ADJ
eurjchem-267	110	3	was	be	AUX
eurjchem-267	110	4	triturated	triturate	VERB
eurjchem-267	110	5	with	with	ADP
eurjchem-267	110	6	benzene	benzene	NOUN
eurjchem-267	110	7	to	to	PART
eurjchem-267	110	8	afford	afford	VERB
eurjchem-267	110	9	a	a	DET
eurjchem-267	110	10	solid	solid	ADJ
eurjchem-267	110	11	product	product	NOUN
eurjchem-267	110	12	which	which	PRON
eurjchem-267	110	13	filtered	filter	VERB
eurjchem-267	110	14	off	off	ADP
eurjchem-267	110	15	,	,	PUNCT
eurjchem-267	110	16	dried	dry	VERB
eurjchem-267	110	17	and	and	CCONJ
eurjchem-267	110	18	recrystallized	recrystallize	VERB
eurjchem-267	110	19	from	from	ADP
eurjchem-267	110	20	dioxane	dioxane	NOUN
eurjchem-267	110	21	to	to	PART
eurjchem-267	110	22	give	give	VERB
eurjchem-267	110	23	7	7	NUM
eurjchem-267	110	24	as	as	ADP
eurjchem-267	110	25	yellow	yellow	ADJ
eurjchem-267	110	26	crystals	crystal	NOUN
eurjchem-267	110	27	(	(	PUNCT
eurjchem-267	110	28	scheme	scheme	NOUN
eurjchem-267	110	29	3	3	NUM
eurjchem-267	110	30	)	)	PUNCT
eurjchem-267	110	31	.	.	PUNCT
eurjchem-267	111	1	yield	yield	NOUN
eurjchem-267	111	2	:	:	PUNCT
eurjchem-267	111	3	62.4	62.4	NUM
eurjchem-267	111	4	%	%	NOUN
eurjchem-267	111	5	.	.	PUNCT
eurjchem-267	112	1	m.p	m.p	PROPN
eurjchem-267	112	2	.	.	PROPN
eurjchem-267	112	3	:	:	PUNCT
eurjchem-267	113	1	147‐149	147‐149	NUM
eurjchem-267	113	2	oc	oc	NOUN
eurjchem-267	113	3	.	.	PUNCT
eurjchem-267	113	4	ft‐ir	ft‐ir	NOUN
eurjchem-267	113	5	(	(	PUNCT
eurjchem-267	113	6	kbr	kbr	PROPN
eurjchem-267	113	7	,	,	PUNCT
eurjchem-267	113	8	cm‐1	cm‐1	PROPN
eurjchem-267	113	9	):	):	PUNCT
eurjchem-267	113	10	3286	3286	NUM
eurjchem-267	113	11	ν(nh	ν(nh	NOUN
eurjchem-267	113	12	)	)	PUNCT
eurjchem-267	113	13	,	,	PUNCT
eurjchem-267	113	14	1716	1716	NUM
eurjchem-267	113	15	ν(c	ν(c	NOUN
eurjchem-267	113	16	=	=	SYM
eurjchem-267	113	17	o	o	NOUN
eurjchem-267	113	18	)	)	PUNCT
eurjchem-267	113	19	,	,	PUNCT
eurjchem-267	113	20	1643	1643	NUM
eurjchem-267	113	21	ν(c	ν(c	PROPN
eurjchem-267	113	22	=	=	SYM
eurjchem-267	113	23	n	n	NUM
eurjchem-267	113	24	)	)	PUNCT
eurjchem-267	113	25	.	.	PUNCT
eurjchem-267	114	1	1h	1h	NUM
eurjchem-267	114	2	nmr	nmr	NOUN
eurjchem-267	114	3	(	(	PUNCT
eurjchem-267	114	4	200	200	NUM
eurjchem-267	114	5	mhz	mhz	NOUN
eurjchem-267	114	6	,	,	PUNCT
eurjchem-267	114	7	cdcl3	cdcl3	NOUN
eurjchem-267	114	8	):	):	PUNCT
eurjchem-267	114	9	8.9	8.9	NUM
eurjchem-267	114	10	(	(	PUNCT
eurjchem-267	114	11	br.s	br.s	PROPN
eurjchem-267	114	12	,	,	PUNCT
eurjchem-267	114	13	1h	1h	NUM
eurjchem-267	114	14	,	,	PUNCT
eurjchem-267	114	15	exchangeable	exchangeable	ADJ
eurjchem-267	114	16	with	with	ADP
eurjchem-267	114	17	d2o	d2o	NOUN
eurjchem-267	114	18	)	)	PUNCT
eurjchem-267	114	19	,	,	PUNCT
eurjchem-267	114	20	8.1‐7.0	8.1‐7.0	NUM
eurjchem-267	114	21	(	(	PUNCT
eurjchem-267	114	22	m	m	PROPN
eurjchem-267	114	23	,	,	PUNCT
eurjchem-267	114	24	14harom	14harom	NUM
eurjchem-267	114	25	.	.	PUNCT
eurjchem-267	114	26	)	)	PUNCT
eurjchem-267	114	27	,	,	PUNCT
eurjchem-267	114	28	6.8	6.8	NUM
eurjchem-267	114	29	(	(	PUNCT
eurjchem-267	114	30	br.s	br.s	PROPN
eurjchem-267	114	31	,	,	PUNCT
eurjchem-267	114	32	3h	3h	NUM
eurjchem-267	114	33	)	)	PUNCT
eurjchem-267	114	34	.	.	PUNCT
eurjchem-267	115	1	ms	ms	NOUN
eurjchem-267	115	2	(	(	PUNCT
eurjchem-267	115	3	ei	ei	PROPN
eurjchem-267	115	4	,	,	PUNCT
eurjchem-267	115	5	m	m	PROPN
eurjchem-267	115	6	/	/	SYM
eurjchem-267	115	7	z	z	PROPN
eurjchem-267	115	8	(	(	PUNCT
eurjchem-267	115	9	%	%	NOUN
eurjchem-267	115	10	)	)	PUNCT
eurjchem-267	115	11	):	):	PUNCT
eurjchem-267	115	12	390	390	NUM
eurjchem-267	115	13	(	(	PUNCT
eurjchem-267	115	14	m+	m+	NOUN
eurjchem-267	115	15	.	.	PROPN
eurjchem-267	115	16	,	,	PUNCT
eurjchem-267	115	17	22.1	22.1	NUM
eurjchem-267	115	18	)	)	PUNCT
eurjchem-267	115	19	,	,	PUNCT
eurjchem-267	115	20	313	313	NUM
eurjchem-267	115	21	(	(	PUNCT
eurjchem-267	115	22	16.7	16.7	NUM
eurjchem-267	115	23	)	)	PUNCT
eurjchem-267	115	24	,	,	PUNCT
eurjchem-267	115	25	287	287	NUM
eurjchem-267	115	26	(	(	PUNCT
eurjchem-267	115	27	23.4	23.4	NUM
eurjchem-267	115	28	)	)	PUNCT
eurjchem-267	115	29	,	,	PUNCT
eurjchem-267	115	30	161	161	NUM
eurjchem-267	115	31	(	(	PUNCT
eurjchem-267	115	32	100	100	NUM
eurjchem-267	115	33	)	)	PUNCT
eurjchem-267	115	34	,	,	PUNCT
eurjchem-267	115	35	77	77	NUM
eurjchem-267	115	36	(	(	PUNCT
eurjchem-267	115	37	48.3	48.3	NUM
eurjchem-267	115	38	)	)	PUNCT
eurjchem-267	115	39	.	.	PUNCT
eurjchem-267	116	1	anal	anal	PROPN
eurjchem-267	116	2	.	.	PUNCT
eurjchem-267	116	3	calcd	calcd	NOUN
eurjchem-267	116	4	.	.	PUNCT
eurjchem-267	117	1	for	for	ADP
eurjchem-267	117	2	c25h18n4o	c25h18n4o	NOUN
eurjchem-267	117	3	(	(	PUNCT
eurjchem-267	117	4	390	390	NUM
eurjchem-267	117	5	):	):	PUNCT
eurjchem-267	117	6	c	c	X
eurjchem-267	117	7	,	,	PUNCT
eurjchem-267	117	8	76.92;	76.92;	PROPN
eurjchem-267	117	9	h	h	NOUN
eurjchem-267	117	10	,	,	PUNCT
eurjchem-267	117	11	4.61	4.61	NUM
eurjchem-267	117	12	;	;	PUNCT
eurjchem-267	117	13	n	n	CCONJ
eurjchem-267	117	14	,	,	PUNCT
eurjchem-267	117	15	14.35	14.35	NUM
eurjchem-267	117	16	.	.	PUNCT
eurjchem-267	118	1	found	find	VERB
eurjchem-267	118	2	:	:	PUNCT
eurjchem-267	119	1	c	c	X
eurjchem-267	119	2	,	,	PUNCT
eurjchem-267	119	3	77.04	77.04	NUM
eurjchem-267	119	4	;	;	PUNCT
eurjchem-267	119	5	h	h	NOUN
eurjchem-267	119	6	,	,	PUNCT
eurjchem-267	119	7	4.93	4.93	NUM
eurjchem-267	119	8	;	;	PUNCT
eurjchem-267	119	9	n	n	CCONJ
eurjchem-267	119	10	,	,	PUNCT
eurjchem-267	119	11	14.66	14.66	NUM
eurjchem-267	119	12	%	%	NOUN
eurjchem-267	119	13	.	.	PUNCT
eurjchem-267	120	1	mahmoud	mahmoud	PROPN
eurjchem-267	120	2	et	et	PROPN
eurjchem-267	120	3	al	al	PROPN
eurjchem-267	120	4	.	.	PUNCT
eurjchem-267	120	5	/	/	SYM
eurjchem-267	120	6	european	european	PROPN
eurjchem-267	120	7	journal	journal	PROPN
eurjchem-267	120	8	of	of	ADP
eurjchem-267	120	9	chemistry	chemistry	NOUN
eurjchem-267	120	10	2	2	NUM
eurjchem-267	120	11	(	(	PUNCT
eurjchem-267	120	12	3	3	NUM
eurjchem-267	120	13	)	)	PUNCT
eurjchem-267	120	14	(	(	PUNCT
eurjchem-267	120	15	2011	2011	NUM
eurjchem-267	120	16	)	)	PUNCT
eurjchem-267	120	17	404‐409	404‐409	NUM
eurjchem-267	120	18	407	407	NUM
eurjchem-267	120	19	n	n	SYM
eurjchem-267	120	20	2	2	NUM
eurjchem-267	120	21	h	h	NOUN
eurjchem-267	120	22	4	4	NUM
eurjchem-267	120	23	.	.	PUNCT
eurjchem-267	120	24	h	h	NOUN
eurjchem-267	121	1	2	2	NUM
eurjchem-267	121	2	o	o	NOUN
eurjchem-267	121	3	st	st	PROPN
eurjchem-267	121	4	ir	ir	PROPN
eurjchem-267	121	5	.	.	PUNCT
eurjchem-267	122	1	r.t	r.t	PROPN
eurjchem-267	122	2	.	.	PUNCT
eurjchem-267	122	3	nh	nh	PROPN
eurjchem-267	122	4	2	2	NUM
eurjchem-267	122	5	oh.hcl	oh.hcl	PROPN
eurjchem-267	122	6	scheme	scheme	NOUN
eurjchem-267	122	7	3	3	NUM
eurjchem-267	122	8	2.9	2.9	NUM
eurjchem-267	122	9	.	.	PUNCT
eurjchem-267	123	1	3‐hydroxy‐2‐[(1z,3e)‐1‐benzamido‐4‐phenyl‐1,3‐	3‐hydroxy‐2‐[(1z,3e)‐1‐benzamido‐4‐phenyl‐1,3‐	NUM
eurjchem-267	123	2	butadien‐1‐yl]quinazolin‐4(h)‐one	butadien‐1‐yl]quinazolin‐4(h)‐one	NUM
eurjchem-267	123	3	(	(	PUNCT
eurjchem-267	123	4	8)	8)	NUM
eurjchem-267	123	5	a	a	DET
eurjchem-267	123	6	mixture	mixture	NOUN
eurjchem-267	123	7	of	of	ADP
eurjchem-267	123	8	1	1	NUM
eurjchem-267	123	9	(	(	PUNCT
eurjchem-267	123	10	0.01	0.01	NUM
eurjchem-267	123	11	mol	mol	NOUN
eurjchem-267	123	12	)	)	PUNCT
eurjchem-267	123	13	,	,	PUNCT
eurjchem-267	123	14	hydroxylamine	hydroxylamine	ADJ
eurjchem-267	123	15	hydrochloride	hydrochloride	NOUN
eurjchem-267	123	16	(	(	PUNCT
eurjchem-267	123	17	2.1	2.1	NUM
eurjchem-267	123	18	g	g	NOUN
eurjchem-267	123	19	,	,	PUNCT
eurjchem-267	123	20	0.02	0.02	NUM
eurjchem-267	123	21	mol	mol	NOUN
eurjchem-267	123	22	)	)	PUNCT
eurjchem-267	123	23	in	in	ADP
eurjchem-267	123	24	pyridine	pyridine	NOUN
eurjchem-267	123	25	(	(	PUNCT
eurjchem-267	123	26	30	30	NUM
eurjchem-267	123	27	ml	ml	NOUN
eurjchem-267	123	28	)	)	PUNCT
eurjchem-267	123	29	was	be	AUX
eurjchem-267	123	30	heated	heat	VERB
eurjchem-267	123	31	under	under	ADP
eurjchem-267	123	32	reflux	reflux	NOUN
eurjchem-267	123	33	for	for	ADP
eurjchem-267	123	34	12	12	NUM
eurjchem-267	123	35	hrs	hrs	NOUN
eurjchem-267	123	36	(	(	PUNCT
eurjchem-267	123	37	tlc	tlc	NOUN
eurjchem-267	123	38	)	)	PUNCT
eurjchem-267	123	39	.	.	PUNCT
eurjchem-267	124	1	the	the	DET
eurjchem-267	124	2	cooled	cool	VERB
eurjchem-267	124	3	mixture	mixture	NOUN
eurjchem-267	124	4	was	be	AUX
eurjchem-267	124	5	acidified	acidify	VERB
eurjchem-267	124	6	with	with	ADP
eurjchem-267	124	7	ice	ice	NOUN
eurjchem-267	124	8	cold	cold	PROPN
eurjchem-267	124	9	hydrochloric	hydrochloric	ADJ
eurjchem-267	124	10	acid	acid	NOUN
eurjchem-267	124	11	and	and	CCONJ
eurjchem-267	124	12	the	the	DET
eurjchem-267	124	13	separated	separate	VERB
eurjchem-267	124	14	solid	solid	ADJ
eurjchem-267	124	15	was	be	AUX
eurjchem-267	124	16	filtered	filter	VERB
eurjchem-267	124	17	off	off	ADP
eurjchem-267	124	18	,	,	PUNCT
eurjchem-267	124	19	dried	dry	VERB
eurjchem-267	124	20	and	and	CCONJ
eurjchem-267	124	21	recrystallized	recrystallize	VERB
eurjchem-267	124	22	from	from	ADP
eurjchem-267	124	23	dioxane	dioxane	NOUN
eurjchem-267	124	24	to	to	PART
eurjchem-267	124	25	give	give	VERB
eurjchem-267	124	26	8	8	NUM
eurjchem-267	124	27	as	as	ADP
eurjchem-267	124	28	pale	pale	ADJ
eurjchem-267	124	29	yellow	yellow	ADJ
eurjchem-267	124	30	crystals	crystal	NOUN
eurjchem-267	124	31	(	(	PUNCT
eurjchem-267	124	32	scheme	scheme	NOUN
eurjchem-267	124	33	3	3	NUM
eurjchem-267	124	34	)	)	PUNCT
eurjchem-267	124	35	.	.	PUNCT
eurjchem-267	125	1	yield	yield	NOUN
eurjchem-267	125	2	:	:	PUNCT
eurjchem-267	125	3	43	43	NUM
eurjchem-267	125	4	%	%	NOUN
eurjchem-267	125	5	.	.	PUNCT
eurjchem-267	126	1	m.p	m.p	PROPN
eurjchem-267	126	2	.	.	PROPN
eurjchem-267	126	3	:	:	PUNCT
eurjchem-267	127	1	217‐219	217‐219	NUM
eurjchem-267	127	2	oc	oc	NOUN
eurjchem-267	127	3	.	.	PUNCT
eurjchem-267	127	4	ft‐ir	ft‐ir	NOUN
eurjchem-267	127	5	(	(	PUNCT
eurjchem-267	127	6	kbr	kbr	PROPN
eurjchem-267	127	7	,	,	PUNCT
eurjchem-267	127	8	cm‐1	cm‐1	PROPN
eurjchem-267	127	9	):	):	PUNCT
eurjchem-267	127	10	br	br	NOUN
eurjchem-267	127	11	.	.	PROPN
eurjchem-267	127	12	3436	3436	NUM
eurjchem-267	127	13	,	,	PUNCT
eurjchem-267	127	14	3217	3217	NUM
eurjchem-267	127	15	ν(nh	ν(nh	NOUN
eurjchem-267	127	16	,	,	PUNCT
eurjchem-267	127	17	oh	oh	INTJ
eurjchem-267	127	18	)	)	PUNCT
eurjchem-267	127	19	,	,	PUNCT
eurjchem-267	127	20	1697	1697	NUM
eurjchem-267	127	21	,	,	PUNCT
eurjchem-267	127	22	1672	1672	NUM
eurjchem-267	127	23	ν(c	ν(c	NOUN
eurjchem-267	127	24	=	=	SYM
eurjchem-267	127	25	o	o	NOUN
eurjchem-267	127	26	)	)	PUNCT
eurjchem-267	127	27	,	,	PUNCT
eurjchem-267	127	28	1612	1612	NUM
eurjchem-267	127	29	ν(c	ν(c	PROPN
eurjchem-267	127	30	=	=	SYM
eurjchem-267	127	31	c	c	NOUN
eurjchem-267	127	32	)	)	PUNCT
eurjchem-267	127	33	.	.	PUNCT
eurjchem-267	128	1	1h	1h	NUM
eurjchem-267	128	2	nmr	nmr	NOUN
eurjchem-267	128	3	(	(	PUNCT
eurjchem-267	128	4	200	200	NUM
eurjchem-267	128	5	mhz	mhz	NOUN
eurjchem-267	128	6	,	,	PUNCT
eurjchem-267	128	7	dmso‐d6	dmso‐d6	NUM
eurjchem-267	128	8	):	):	PUNCT
eurjchem-267	128	9	9.3	9.3	NUM
eurjchem-267	128	10	(	(	PUNCT
eurjchem-267	128	11	br.s	br.s	PROPN
eurjchem-267	128	12	,	,	PUNCT
eurjchem-267	128	13	1h	1h	NUM
eurjchem-267	128	14	,	,	PUNCT
eurjchem-267	128	15	exchangeable	exchangeable	ADJ
eurjchem-267	128	16	with	with	ADP
eurjchem-267	128	17	d2o	d2o	NOUN
eurjchem-267	128	18	)	)	PUNCT
eurjchem-267	128	19	,	,	PUNCT
eurjchem-267	128	20	8.6	8.6	NUM
eurjchem-267	128	21	(	(	PUNCT
eurjchem-267	128	22	br.s	br.s	PROPN
eurjchem-267	128	23	,	,	PUNCT
eurjchem-267	128	24	1h	1h	NUM
eurjchem-267	128	25	,	,	PUNCT
eurjchem-267	128	26	exchangeable	exchangeable	ADJ
eurjchem-267	128	27	with	with	ADP
eurjchem-267	128	28	d2o	d2o	NOUN
eurjchem-267	128	29	)	)	PUNCT
eurjchem-267	128	30	,	,	PUNCT
eurjchem-267	128	31	7.9‐7.0	7.9‐7.0	NUM
eurjchem-267	128	32	(	(	PUNCT
eurjchem-267	128	33	m	m	PROPN
eurjchem-267	128	34	,	,	PUNCT
eurjchem-267	128	35	14harom	14harom	NUM
eurjchem-267	128	36	.	.	PUNCT
eurjchem-267	128	37	)	)	PUNCT
eurjchem-267	128	38	,	,	PUNCT
eurjchem-267	128	39	6.7	6.7	NUM
eurjchem-267	128	40	(	(	PUNCT
eurjchem-267	128	41	br.s	br.s	PROPN
eurjchem-267	128	42	,	,	PUNCT
eurjchem-267	128	43	3h	3h	NUM
eurjchem-267	128	44	)	)	PUNCT
eurjchem-267	128	45	.	.	PUNCT
eurjchem-267	129	1	ms	ms	NOUN
eurjchem-267	129	2	(	(	PUNCT
eurjchem-267	129	3	ei	ei	PROPN
eurjchem-267	129	4	,	,	PUNCT
eurjchem-267	129	5	m	m	PROPN
eurjchem-267	129	6	/	/	SYM
eurjchem-267	129	7	z	z	PROPN
eurjchem-267	129	8	(	(	PUNCT
eurjchem-267	129	9	%	%	NOUN
eurjchem-267	129	10	)	)	PUNCT
eurjchem-267	129	11	):	):	PUNCT
eurjchem-267	129	12	409	409	NUM
eurjchem-267	129	13	(	(	PUNCT
eurjchem-267	129	14	m+	m+	NUM
eurjchem-267	129	15	.	.	PROPN
eurjchem-267	129	16	,	,	PUNCT
eurjchem-267	129	17	21.3	21.3	NUM
eurjchem-267	129	18	)	)	PUNCT
eurjchem-267	129	19	,	,	PUNCT
eurjchem-267	129	20	392	392	NUM
eurjchem-267	129	21	(	(	PUNCT
eurjchem-267	129	22	76.3	76.3	NUM
eurjchem-267	129	23	)	)	PUNCT
eurjchem-267	129	24	,	,	PUNCT
eurjchem-267	129	25	105	105	NUM
eurjchem-267	129	26	(	(	PUNCT
eurjchem-267	129	27	100	100	NUM
eurjchem-267	129	28	)	)	PUNCT
eurjchem-267	129	29	,	,	PUNCT
eurjchem-267	129	30	77	77	NUM
eurjchem-267	129	31	(	(	PUNCT
eurjchem-267	129	32	66.3	66.3	NUM
eurjchem-267	129	33	)	)	PUNCT
eurjchem-267	129	34	.	.	PUNCT
eurjchem-267	130	1	anal	anal	PROPN
eurjchem-267	130	2	.	.	PUNCT
eurjchem-267	130	3	calcd	calcd	NOUN
eurjchem-267	130	4	.	.	PUNCT
eurjchem-267	131	1	for	for	ADP
eurjchem-267	131	2	c25h19n3o3	c25h19n3o3	NOUN
eurjchem-267	131	3	(	(	PUNCT
eurjchem-267	131	4	409	409	NUM
eurjchem-267	131	5	):	):	PUNCT
eurjchem-267	131	6	c	c	NOUN
eurjchem-267	131	7	,	,	PUNCT
eurjchem-267	131	8	73.34;	73.34;	PROPN
eurjchem-267	131	9	h	h	NOUN
eurjchem-267	131	10	,	,	PUNCT
eurjchem-267	131	11	4.64	4.64	NUM
eurjchem-267	131	12	;	;	PUNCT
eurjchem-267	131	13	n	n	CCONJ
eurjchem-267	131	14	,	,	PUNCT
eurjchem-267	131	15	10.26	10.26	NUM
eurjchem-267	131	16	.	.	PUNCT
eurjchem-267	131	17	found	find	VERB
eurjchem-267	131	18	:	:	PUNCT
eurjchem-267	132	1	c	c	X
eurjchem-267	132	2	,	,	PUNCT
eurjchem-267	132	3	73.08	73.08	NUM
eurjchem-267	132	4	;	;	PUNCT
eurjchem-267	132	5	h	h	NOUN
eurjchem-267	132	6	,	,	PUNCT
eurjchem-267	132	7	4.63	4.63	NUM
eurjchem-267	132	8	;	;	PUNCT
eurjchem-267	132	9	n	n	CCONJ
eurjchem-267	132	10	,	,	PUNCT
eurjchem-267	132	11	10.17	10.17	NUM
eurjchem-267	132	12	%	%	NOUN
eurjchem-267	132	13	.	.	PUNCT
eurjchem-267	133	1	2.10	2.10	NUM
eurjchem-267	133	2	.	.	PUNCT
eurjchem-267	134	1	1,2,5‐oxadiazino[3,2‐b]quinazolin‐10(4h)‐one	1,2,5‐oxadiazino[3,2‐b]quinazolin‐10(4h)‐one	NUM
eurjchem-267	134	2	derivative	derivative	NOUN
eurjchem-267	134	3	(	(	PUNCT
eurjchem-267	134	4	9	9	NUM
eurjchem-267	134	5	)	)	PUNCT
eurjchem-267	134	6	compound	compound	NOUN
eurjchem-267	134	7	8	8	NUM
eurjchem-267	134	8	(	(	PUNCT
eurjchem-267	134	9	1	1	NUM
eurjchem-267	134	10	g	g	NOUN
eurjchem-267	134	11	,	,	PUNCT
eurjchem-267	134	12	0.002	0.002	NUM
eurjchem-267	134	13	mol	mol	NOUN
eurjchem-267	134	14	)	)	PUNCT
eurjchem-267	134	15	and	and	CCONJ
eurjchem-267	134	16	freshly	freshly	ADV
eurjchem-267	134	17	distilled	distil	VERB
eurjchem-267	134	18	acetic	acetic	ADJ
eurjchem-267	134	19	anhydride	anhydride	NOUN
eurjchem-267	134	20	(	(	PUNCT
eurjchem-267	134	21	10	10	NUM
eurjchem-267	134	22	ml	ml	NOUN
eurjchem-267	134	23	)	)	PUNCT
eurjchem-267	134	24	was	be	AUX
eurjchem-267	134	25	heated	heat	VERB
eurjchem-267	134	26	under	under	ADP
eurjchem-267	134	27	reflux	reflux	NOUN
eurjchem-267	134	28	for	for	ADP
eurjchem-267	134	29	2	2	NUM
eurjchem-267	134	30	hrs	hrs	NOUN
eurjchem-267	134	31	(	(	PUNCT
eurjchem-267	134	32	tlc	tlc	NOUN
eurjchem-267	134	33	)	)	PUNCT
eurjchem-267	134	34	.	.	PUNCT
eurjchem-267	135	1	the	the	DET
eurjchem-267	135	2	cooled	cool	VERB
eurjchem-267	135	3	reaction	reaction	NOUN
eurjchem-267	135	4	mixture	mixture	NOUN
eurjchem-267	135	5	was	be	AUX
eurjchem-267	135	6	poured	pour	VERB
eurjchem-267	135	7	onto	onto	ADP
eurjchem-267	135	8	ice‐water	ice‐water	NOUN
eurjchem-267	135	9	and	and	CCONJ
eurjchem-267	135	10	stirred	stir	VERB
eurjchem-267	135	11	for	for	ADP
eurjchem-267	135	12	0.5	0.5	NUM
eurjchem-267	135	13	hr	hr	NOUN
eurjchem-267	135	14	and	and	CCONJ
eurjchem-267	135	15	the	the	DET
eurjchem-267	135	16	crude	crude	ADJ
eurjchem-267	135	17	solid	solid	ADJ
eurjchem-267	135	18	obtained	obtain	VERB
eurjchem-267	135	19	was	be	AUX
eurjchem-267	135	20	filtered	filter	VERB
eurjchem-267	135	21	off	off	ADP
eurjchem-267	135	22	,	,	PUNCT
eurjchem-267	135	23	dried	dry	VERB
eurjchem-267	135	24	and	and	CCONJ
eurjchem-267	135	25	recrystallized	recrystallize	VERB
eurjchem-267	135	26	from	from	ADP
eurjchem-267	135	27	dioxane	dioxane	NOUN
eurjchem-267	135	28	to	to	PART
eurjchem-267	135	29	give	give	VERB
eurjchem-267	135	30	9	9	NUM
eurjchem-267	135	31	as	as	ADP
eurjchem-267	135	32	a	a	DET
eurjchem-267	135	33	light	light	ADJ
eurjchem-267	135	34	brown	brown	ADJ
eurjchem-267	135	35	crystals	crystal	NOUN
eurjchem-267	135	36	(	(	PUNCT
eurjchem-267	135	37	scheme	scheme	NOUN
eurjchem-267	135	38	3	3	NUM
eurjchem-267	135	39	)	)	PUNCT
eurjchem-267	135	40	.	.	PUNCT
eurjchem-267	136	1	yield	yield	NOUN
eurjchem-267	136	2	:	:	PUNCT
eurjchem-267	136	3	0.68	0.68	NUM
eurjchem-267	136	4	g	g	NOUN
eurjchem-267	136	5	,	,	PUNCT
eurjchem-267	136	6	71.5	71.5	NUM
eurjchem-267	136	7	%	%	NOUN
eurjchem-267	136	8	.	.	PUNCT
eurjchem-267	137	1	m.p	m.p	PROPN
eurjchem-267	137	2	.	.	PROPN
eurjchem-267	137	3	:	:	PUNCT
eurjchem-267	138	1	194‐196	194‐196	NUM
eurjchem-267	138	2	oc	oc	X
eurjchem-267	138	3	.	.	PUNCT
eurjchem-267	139	1	ft‐	ft‐	PROPN
eurjchem-267	139	2	ir	ir	PROPN
eurjchem-267	139	3	(	(	PUNCT
eurjchem-267	139	4	kbr	kbr	PROPN
eurjchem-267	139	5	,	,	PUNCT
eurjchem-267	139	6	cm‐1	cm‐1	PROPN
eurjchem-267	139	7	):	):	PUNCT
eurjchem-267	139	8	1731	1731	NUM
eurjchem-267	139	9	ν(c	ν(c	NOUN
eurjchem-267	139	10	=	=	SYM
eurjchem-267	139	11	o	o	NOUN
eurjchem-267	139	12	)	)	PUNCT
eurjchem-267	139	13	,	,	PUNCT
eurjchem-267	139	14	1634	1634	NUM
eurjchem-267	139	15	ν(c	ν(c	PROPN
eurjchem-267	139	16	=	=	SYM
eurjchem-267	139	17	n	n	NUM
eurjchem-267	139	18	)	)	PUNCT
eurjchem-267	139	19	,	,	PUNCT
eurjchem-267	139	20	1610	1610	NUM
eurjchem-267	139	21	ν(c	ν(c	PROPN
eurjchem-267	139	22	=	=	SYM
eurjchem-267	139	23	c	c	NOUN
eurjchem-267	139	24	)	)	PUNCT
eurjchem-267	139	25	,	,	PUNCT
eurjchem-267	139	26	980	980	NUM
eurjchem-267	139	27	,	,	PUNCT
eurjchem-267	139	28	940	940	NUM
eurjchem-267	139	29	ν(no	ν(no	PROPN
eurjchem-267	139	30	)	)	PUNCT
eurjchem-267	139	31	.	.	PUNCT
eurjchem-267	140	1	1h	1h	NUM
eurjchem-267	140	2	nmr	nmr	NOUN
eurjchem-267	140	3	(	(	PUNCT
eurjchem-267	140	4	200	200	NUM
eurjchem-267	140	5	mhz	mhz	NOUN
eurjchem-267	140	6	,	,	PUNCT
eurjchem-267	140	7	cdcl3	cdcl3	NOUN
eurjchem-267	140	8	):	):	PUNCT
eurjchem-267	140	9	8.1‐7.3	8.1‐7.3	NUM
eurjchem-267	140	10	(	(	PUNCT
eurjchem-267	140	11	m	m	PROPN
eurjchem-267	140	12	,	,	PUNCT
eurjchem-267	140	13	14harom	14harom	NUM
eurjchem-267	140	14	.	.	PUNCT
eurjchem-267	140	15	)	)	PUNCT
eurjchem-267	140	16	,	,	PUNCT
eurjchem-267	140	17	6.9‐	6.9‐	NUM
eurjchem-267	140	18	6.6	6.6	NUM
eurjchem-267	140	19	(	(	PUNCT
eurjchem-267	140	20	m	m	PROPN
eurjchem-267	140	21	,	,	PUNCT
eurjchem-267	140	22	3h	3h	NUM
eurjchem-267	140	23	)	)	PUNCT
eurjchem-267	140	24	.	.	PUNCT
eurjchem-267	141	1	ms	ms	NOUN
eurjchem-267	141	2	(	(	PUNCT
eurjchem-267	141	3	ei	ei	PROPN
eurjchem-267	141	4	,	,	PUNCT
eurjchem-267	141	5	m	m	PROPN
eurjchem-267	141	6	/	/	SYM
eurjchem-267	141	7	z	z	PROPN
eurjchem-267	141	8	(	(	PUNCT
eurjchem-267	141	9	%	%	NOUN
eurjchem-267	141	10	)	)	PUNCT
eurjchem-267	141	11	):	):	PUNCT
eurjchem-267	141	12	391	391	NUM
eurjchem-267	141	13	(	(	PUNCT
eurjchem-267	141	14	m+	m+	NUM
eurjchem-267	141	15	.	.	PROPN
eurjchem-267	141	16	,	,	PUNCT
eurjchem-267	141	17	17.3	17.3	NUM
eurjchem-267	141	18	)	)	PUNCT
eurjchem-267	141	19	,	,	PUNCT
eurjchem-267	141	20	314	314	NUM
eurjchem-267	141	21	(	(	PUNCT
eurjchem-267	141	22	41.2	41.2	NUM
eurjchem-267	141	23	)	)	PUNCT
eurjchem-267	141	24	,	,	PUNCT
eurjchem-267	141	25	288	288	NUM
eurjchem-267	141	26	(	(	PUNCT
eurjchem-267	141	27	100	100	NUM
eurjchem-267	141	28	)	)	PUNCT
eurjchem-267	141	29	,	,	PUNCT
eurjchem-267	141	30	77	77	NUM
eurjchem-267	141	31	(	(	PUNCT
eurjchem-267	141	32	36.1	36.1	NUM
eurjchem-267	141	33	)	)	PUNCT
eurjchem-267	141	34	.	.	PUNCT
eurjchem-267	142	1	anal	anal	PROPN
eurjchem-267	142	2	.	.	PUNCT
eurjchem-267	142	3	calcd	calcd	NOUN
eurjchem-267	142	4	.	.	PUNCT
eurjchem-267	143	1	for	for	SCONJ
eurjchem-267	143	2	c25h17n3o2	c25h17n3o2	PROPN
eurjchem-267	143	3	(	(	PUNCT
eurjchem-267	143	4	391	391	NUM
eurjchem-267	143	5	):	):	PUNCT
eurjchem-267	143	6	c	c	X
eurjchem-267	143	7	,	,	PUNCT
eurjchem-267	143	8	76.72;	76.72;	NUM
eurjchem-267	143	9	h	h	NOUN
eurjchem-267	143	10	,	,	PUNCT
eurjchem-267	143	11	4.34	4.34	NUM
eurjchem-267	143	12	;	;	PUNCT
eurjchem-267	143	13	n	n	CCONJ
eurjchem-267	143	14	,	,	PUNCT
eurjchem-267	143	15	10.74	10.74	NUM
eurjchem-267	143	16	.	.	PUNCT
eurjchem-267	143	17	found	find	VERB
eurjchem-267	143	18	:	:	PUNCT
eurjchem-267	144	1	c	c	X
eurjchem-267	144	2	,	,	PUNCT
eurjchem-267	144	3	76.33	76.33	NUM
eurjchem-267	144	4	;	;	PUNCT
eurjchem-267	144	5	h	h	NOUN
eurjchem-267	144	6	,	,	PUNCT
eurjchem-267	144	7	4.08	4.08	NUM
eurjchem-267	144	8	;	;	PUNCT
eurjchem-267	144	9	n	n	CCONJ
eurjchem-267	144	10	,	,	PUNCT
eurjchem-267	144	11	10.47	10.47	NUM
eurjchem-267	144	12	%	%	NOUN
eurjchem-267	144	13	.	.	PUNCT
eurjchem-267	145	1	2.11	2.11	NUM
eurjchem-267	145	2	.	.	X
eurjchem-267	145	3	3‐(4‐aminobiphenyl‐4‐yl)‐2‐[(1z,3e)‐1‐benzamido‐4‐	3‐(4‐aminobiphenyl‐4‐yl)‐2‐[(1z,3e)‐1‐benzamido‐4‐	NUM
eurjchem-267	145	4	phenyl‐1,3‐butadien‐1‐yl]quinazolin‐4(h)‐one	phenyl‐1,3‐butadien‐1‐yl]quinazolin‐4(h)‐one	NOUN
eurjchem-267	145	5	(	(	PUNCT
eurjchem-267	145	6	10	10	NUM
eurjchem-267	145	7	)	)	PUNCT
eurjchem-267	145	8	a	a	DET
eurjchem-267	145	9	mixture	mixture	NOUN
eurjchem-267	145	10	of	of	ADP
eurjchem-267	145	11	1	1	NUM
eurjchem-267	145	12	(	(	PUNCT
eurjchem-267	145	13	1.2	1.2	NUM
eurjchem-267	145	14	g	g	NOUN
eurjchem-267	145	15	,	,	PUNCT
eurjchem-267	145	16	0.003	0.003	NUM
eurjchem-267	145	17	mol	mol	NOUN
eurjchem-267	145	18	)	)	PUNCT
eurjchem-267	145	19	and	and	CCONJ
eurjchem-267	145	20	benzidine	benzidine	NOUN
eurjchem-267	145	21	(	(	PUNCT
eurjchem-267	145	22	0.55	0.55	NUM
eurjchem-267	145	23	g	g	NOUN
eurjchem-267	145	24	,	,	PUNCT
eurjchem-267	145	25	0.003	0.003	NUM
eurjchem-267	145	26	mol	mol	NOUN
eurjchem-267	145	27	)	)	PUNCT
eurjchem-267	145	28	in	in	ADP
eurjchem-267	145	29	n‐butanol	n‐butanol	PROPN
eurjchem-267	145	30	(	(	PUNCT
eurjchem-267	145	31	30	30	NUM
eurjchem-267	145	32	ml	ml	NOUN
eurjchem-267	145	33	)	)	PUNCT
eurjchem-267	145	34	was	be	AUX
eurjchem-267	145	35	refluxed	refluxe	VERB
eurjchem-267	145	36	for	for	ADP
eurjchem-267	145	37	12	12	NUM
eurjchem-267	145	38	hrs	hrs	NOUN
eurjchem-267	145	39	(	(	PUNCT
eurjchem-267	145	40	tlc	tlc	NOUN
eurjchem-267	145	41	)	)	PUNCT
eurjchem-267	145	42	.	.	PUNCT
eurjchem-267	146	1	the	the	DET
eurjchem-267	146	2	reaction	reaction	NOUN
eurjchem-267	146	3	mixture	mixture	NOUN
eurjchem-267	146	4	was	be	AUX
eurjchem-267	146	5	concentrated	concentrate	VERB
eurjchem-267	146	6	and	and	CCONJ
eurjchem-267	146	7	the	the	DET
eurjchem-267	146	8	solid	solid	ADJ
eurjchem-267	146	9	separated	separate	VERB
eurjchem-267	146	10	after	after	SCONJ
eurjchem-267	146	11	cooling	cool	VERB
eurjchem-267	146	12	was	be	AUX
eurjchem-267	146	13	filtered	filter	VERB
eurjchem-267	146	14	off	off	ADP
eurjchem-267	146	15	,	,	PUNCT
eurjchem-267	146	16	washed	wash	VERB
eurjchem-267	146	17	several	several	ADJ
eurjchem-267	146	18	times	time	NOUN
eurjchem-267	146	19	with	with	ADP
eurjchem-267	146	20	diluted	diluted	ADJ
eurjchem-267	146	21	methanol	methanol	NOUN
eurjchem-267	146	22	,	,	PUNCT
eurjchem-267	146	23	dried	dry	VERB
eurjchem-267	146	24	and	and	CCONJ
eurjchem-267	146	25	recrystallized	recrystallize	VERB
eurjchem-267	146	26	from	from	ADP
eurjchem-267	146	27	ethanol	ethanol	NOUN
eurjchem-267	146	28	to	to	PART
eurjchem-267	146	29	give	give	VERB
eurjchem-267	146	30	10	10	NUM
eurjchem-267	146	31	as	as	ADP
eurjchem-267	146	32	a	a	DET
eurjchem-267	146	33	yellowish‐green	yellowish‐green	NUM
eurjchem-267	146	34	crystals	crystal	NOUN
eurjchem-267	146	35	(	(	PUNCT
eurjchem-267	146	36	scheme	scheme	NOUN
eurjchem-267	146	37	3	3	NUM
eurjchem-267	146	38	)	)	PUNCT
eurjchem-267	146	39	.	.	PUNCT
eurjchem-267	147	1	yield	yield	NOUN
eurjchem-267	147	2	:	:	PUNCT
eurjchem-267	147	3	72	72	NUM
eurjchem-267	147	4	%	%	NOUN
eurjchem-267	147	5	.	.	PUNCT
eurjchem-267	148	1	m.p	m.p	PROPN
eurjchem-267	148	2	.	.	PROPN
eurjchem-267	148	3	:	:	PUNCT
eurjchem-267	149	1	130‐132	130‐132	NUM
eurjchem-267	149	2	oc	oc	PROPN
eurjchem-267	149	3	.	.	PUNCT
eurjchem-267	149	4	ft‐ir	ft‐ir	NOUN
eurjchem-267	149	5	(	(	PUNCT
eurjchem-267	149	6	kbr	kbr	PROPN
eurjchem-267	149	7	,	,	PUNCT
eurjchem-267	149	8	cm‐1	cm‐1	PROPN
eurjchem-267	149	9	):	):	PUNCT
eurjchem-267	149	10	br	br	PROPN
eurjchem-267	149	11	.	.	PUNCT
eurjchem-267	149	12	centered	center	VERB
eurjchem-267	149	13	at	at	ADP
eurjchem-267	149	14	3358	3358	NUM
eurjchem-267	149	15	ν(nh2	ν(nh2	PROPN
eurjchem-267	149	16	)	)	PUNCT
eurjchem-267	149	17	,	,	PUNCT
eurjchem-267	149	18	1742	1742	NUM
eurjchem-267	149	19	ν(c	ν(c	PROPN
eurjchem-267	149	20	=	=	SYM
eurjchem-267	149	21	o	o	NOUN
eurjchem-267	149	22	)	)	PUNCT
eurjchem-267	149	23	,	,	PUNCT
eurjchem-267	149	24	1692	1692	NUM
eurjchem-267	149	25	ν(c	ν(c	PROPN
eurjchem-267	149	26	=	=	SYM
eurjchem-267	149	27	o	o	NOUN
eurjchem-267	149	28	)	)	PUNCT
eurjchem-267	149	29	,	,	PUNCT
eurjchem-267	149	30	1621	1621	NUM
eurjchem-267	149	31	ν(c	ν(c	PROPN
eurjchem-267	149	32	=	=	SYM
eurjchem-267	149	33	n	n	NUM
eurjchem-267	149	34	)	)	PUNCT
eurjchem-267	149	35	.	.	PUNCT
eurjchem-267	150	1	1h	1h	NUM
eurjchem-267	150	2	nmr	nmr	NOUN
eurjchem-267	150	3	(	(	PUNCT
eurjchem-267	150	4	200	200	NUM
eurjchem-267	150	5	mhz	mhz	NOUN
eurjchem-267	150	6	,	,	PUNCT
eurjchem-267	150	7	cdcl3	cdcl3	NOUN
eurjchem-267	150	8	):	):	PUNCT
eurjchem-267	150	9	9.1	9.1	NUM
eurjchem-267	150	10	(	(	PUNCT
eurjchem-267	150	11	br.s	br.s	PROPN
eurjchem-267	150	12	,	,	PUNCT
eurjchem-267	150	13	1h	1h	NUM
eurjchem-267	150	14	,	,	PUNCT
eurjchem-267	150	15	exchangeable	exchangeable	ADJ
eurjchem-267	150	16	with	with	ADP
eurjchem-267	150	17	d2o	d2o	NOUN
eurjchem-267	150	18	)	)	PUNCT
eurjchem-267	150	19	,	,	PUNCT
eurjchem-267	150	20	8.4‐7.3	8.4‐7.3	NUM
eurjchem-267	150	21	(	(	PUNCT
eurjchem-267	150	22	m	m	PROPN
eurjchem-267	150	23	,	,	PUNCT
eurjchem-267	150	24	22harom	22harom	PROPN
eurjchem-267	150	25	.	.	PUNCT
eurjchem-267	150	26	)	)	PUNCT
eurjchem-267	150	27	,	,	PUNCT
eurjchem-267	150	28	6.77	6.77	NUM
eurjchem-267	150	29	(	(	PUNCT
eurjchem-267	150	30	br.s	br.s	PROPN
eurjchem-267	150	31	,	,	PUNCT
eurjchem-267	150	32	3h	3h	NUM
eurjchem-267	150	33	)	)	PUNCT
eurjchem-267	150	34	,	,	PUNCT
eurjchem-267	150	35	4.6	4.6	NUM
eurjchem-267	150	36	(	(	PUNCT
eurjchem-267	150	37	br.s	br.s	PROPN
eurjchem-267	150	38	,	,	PUNCT
eurjchem-267	150	39	2h	2h	NUM
eurjchem-267	150	40	,	,	PUNCT
eurjchem-267	150	41	exchangeable	exchangeable	ADJ
eurjchem-267	150	42	with	with	ADP
eurjchem-267	150	43	d2o	d2o	NOUN
eurjchem-267	150	44	)	)	PUNCT
eurjchem-267	150	45	.	.	PUNCT
eurjchem-267	151	1	ms	ms	NOUN
eurjchem-267	151	2	(	(	PUNCT
eurjchem-267	151	3	ei	ei	PROPN
eurjchem-267	151	4	,	,	PUNCT
eurjchem-267	151	5	m	m	PROPN
eurjchem-267	151	6	/	/	SYM
eurjchem-267	151	7	z	z	PROPN
eurjchem-267	151	8	(	(	PUNCT
eurjchem-267	151	9	%	%	NOUN
eurjchem-267	151	10	)	)	PUNCT
eurjchem-267	151	11	):	):	PUNCT
eurjchem-267	151	12	560	560	NUM
eurjchem-267	151	13	(	(	PUNCT
eurjchem-267	151	14	m+.‐1	m+.‐1	NOUN
eurjchem-267	151	15	,	,	PUNCT
eurjchem-267	151	16	12.9	12.9	NUM
eurjchem-267	151	17	)	)	PUNCT
eurjchem-267	151	18	,	,	PUNCT
eurjchem-267	151	19	313	313	NUM
eurjchem-267	151	20	(	(	PUNCT
eurjchem-267	151	21	10.6	10.6	NUM
eurjchem-267	151	22	)	)	PUNCT
eurjchem-267	151	23	,	,	PUNCT
eurjchem-267	151	24	210	210	NUM
eurjchem-267	151	25	(	(	PUNCT
eurjchem-267	151	26	15	15	NUM
eurjchem-267	151	27	)	)	PUNCT
eurjchem-267	151	28	,	,	PUNCT
eurjchem-267	151	29	184	184	NUM
eurjchem-267	151	30	(	(	PUNCT
eurjchem-267	151	31	28.7	28.7	NUM
eurjchem-267	151	32	)	)	PUNCT
eurjchem-267	151	33	,	,	PUNCT
eurjchem-267	151	34	105	105	NUM
eurjchem-267	151	35	(	(	PUNCT
eurjchem-267	151	36	100	100	NUM
eurjchem-267	151	37	)	)	PUNCT
eurjchem-267	151	38	,	,	PUNCT
eurjchem-267	151	39	77	77	NUM
eurjchem-267	151	40	(	(	PUNCT
eurjchem-267	151	41	70.2	70.2	NUM
eurjchem-267	151	42	)	)	PUNCT
eurjchem-267	151	43	.	.	PUNCT
eurjchem-267	152	1	anal	anal	PROPN
eurjchem-267	152	2	.	.	PUNCT
eurjchem-267	152	3	calcd	calcd	NOUN
eurjchem-267	152	4	.	.	PUNCT
eurjchem-267	153	1	for	for	ADP
eurjchem-267	153	2	c37h28n4o2	c37h28n4o2	PROPN
eurjchem-267	153	3	(	(	PUNCT
eurjchem-267	153	4	561	561	NUM
eurjchem-267	153	5	):	):	PUNCT
eurjchem-267	153	6	c	c	X
eurjchem-267	153	7	,	,	PUNCT
eurjchem-267	153	8	79.14;	79.14;	ADJ
eurjchem-267	153	9	h	h	NOUN
eurjchem-267	153	10	,	,	PUNCT
eurjchem-267	153	11	4.99	4.99	NUM
eurjchem-267	153	12	;	;	PUNCT
eurjchem-267	153	13	n	n	CCONJ
eurjchem-267	153	14	,	,	PUNCT
eurjchem-267	153	15	9.98	9.98	NUM
eurjchem-267	153	16	.	.	PUNCT
eurjchem-267	153	17	found	find	VERB
eurjchem-267	153	18	:	:	PUNCT
eurjchem-267	154	1	c	c	X
eurjchem-267	154	2	,	,	PUNCT
eurjchem-267	154	3	79.08	79.08	NUM
eurjchem-267	154	4	;	;	PUNCT
eurjchem-267	154	5	h	h	NOUN
eurjchem-267	154	6	,	,	PUNCT
eurjchem-267	154	7	4.71	4.71	NUM
eurjchem-267	154	8	;	;	PUNCT
eurjchem-267	154	9	n	n	CCONJ
eurjchem-267	154	10	,	,	PUNCT
eurjchem-267	154	11	10.15	10.15	NUM
eurjchem-267	154	12	%	%	NOUN
eurjchem-267	154	13	.	.	PUNCT
eurjchem-267	155	1	2.12	2.12	NUM
eurjchem-267	155	2	.	.	PUNCT
eurjchem-267	156	1	benzimidazolo[1,2‐c]quinazoline	benzimidazolo[1,2‐c]quinazoline	PROPN
eurjchem-267	156	2	derivative	derivative	NOUN
eurjchem-267	156	3	(	(	PUNCT
eurjchem-267	156	4	11	11	NUM
eurjchem-267	156	5	)	)	PUNCT
eurjchem-267	156	6	a	a	DET
eurjchem-267	156	7	mixture	mixture	NOUN
eurjchem-267	156	8	of	of	ADP
eurjchem-267	156	9	1	1	NUM
eurjchem-267	156	10	(	(	PUNCT
eurjchem-267	156	11	1.2	1.2	NUM
eurjchem-267	156	12	g	g	NOUN
eurjchem-267	156	13	,	,	PUNCT
eurjchem-267	156	14	0.003	0.003	NUM
eurjchem-267	156	15	mol	mol	NOUN
eurjchem-267	156	16	)	)	PUNCT
eurjchem-267	156	17	and	and	CCONJ
eurjchem-267	156	18	o‐phenylenediamine	o‐phenylenediamine	NUM
eurjchem-267	156	19	(	(	PUNCT
eurjchem-267	156	20	0.65	0.65	NUM
eurjchem-267	156	21	g	g	NOUN
eurjchem-267	156	22	,	,	PUNCT
eurjchem-267	156	23	0.006	0.006	NUM
eurjchem-267	156	24	mol	mol	NOUN
eurjchem-267	156	25	)	)	PUNCT
eurjchem-267	156	26	was	be	AUX
eurjchem-267	156	27	heated	heat	VERB
eurjchem-267	156	28	with	with	ADP
eurjchem-267	156	29	stirring	stir	VERB
eurjchem-267	156	30	on	on	ADP
eurjchem-267	156	31	an	an	DET
eurjchem-267	156	32	oil‐bath	oil‐bath	NOUN
eurjchem-267	156	33	for	for	ADP
eurjchem-267	156	34	6	6	NUM
eurjchem-267	156	35	hrs	hrs	NOUN
eurjchem-267	156	36	at	at	ADP
eurjchem-267	156	37	190	190	NUM
eurjchem-267	156	38	oc	oc	NOUN
eurjchem-267	156	39	.	.	PUNCT
eurjchem-267	157	1	the	the	DET
eurjchem-267	157	2	crude	crude	ADJ
eurjchem-267	157	3	product	product	NOUN
eurjchem-267	157	4	was	be	AUX
eurjchem-267	157	5	triturated	triturate	VERB
eurjchem-267	157	6	with	with	ADP
eurjchem-267	157	7	water	water	NOUN
eurjchem-267	157	8	then	then	ADV
eurjchem-267	157	9	filtered	filter	VERB
eurjchem-267	157	10	off	off	ADP
eurjchem-267	157	11	,	,	PUNCT
eurjchem-267	157	12	washed	wash	VERB
eurjchem-267	157	13	several	several	ADJ
eurjchem-267	157	14	times	time	NOUN
eurjchem-267	157	15	with	with	ADP
eurjchem-267	157	16	diethyl	diethyl	NOUN
eurjchem-267	157	17	ether	ether	NOUN
eurjchem-267	157	18	,	,	PUNCT
eurjchem-267	157	19	dried	dry	VERB
eurjchem-267	157	20	and	and	CCONJ
eurjchem-267	157	21	recrystallized	recrystallize	VERB
eurjchem-267	157	22	from	from	ADP
eurjchem-267	157	23	benzene‐ethanol	benzene‐ethanol	NOUN
eurjchem-267	157	24	to	to	PART
eurjchem-267	157	25	give	give	VERB
eurjchem-267	157	26	11	11	NUM
eurjchem-267	157	27	as	as	ADP
eurjchem-267	157	28	a	a	DET
eurjchem-267	157	29	light	light	ADJ
eurjchem-267	157	30	brown	brown	ADJ
eurjchem-267	157	31	crystals	crystal	NOUN
eurjchem-267	157	32	(	(	PUNCT
eurjchem-267	157	33	scheme	scheme	NOUN
eurjchem-267	157	34	3	3	NUM
eurjchem-267	157	35	)	)	PUNCT
eurjchem-267	157	36	.	.	PUNCT
eurjchem-267	158	1	yield	yield	NOUN
eurjchem-267	158	2	:	:	PUNCT
eurjchem-267	158	3	0.86	0.86	NUM
eurjchem-267	158	4	g	g	NOUN
eurjchem-267	158	5	,	,	PUNCT
eurjchem-267	158	6	61.4	61.4	NUM
eurjchem-267	158	7	%	%	NOUN
eurjchem-267	158	8	.	.	PUNCT
eurjchem-267	159	1	m.p	m.p	PROPN
eurjchem-267	159	2	.	.	PROPN
eurjchem-267	159	3	:	:	PUNCT
eurjchem-267	160	1	210‐212	210‐212	NUM
eurjchem-267	160	2	oc	oc	VERB
eurjchem-267	160	3	.	.	PROPN
eurjchem-267	160	4	ir	ir	PROPN
eurjchem-267	160	5	(	(	PUNCT
eurjchem-267	160	6	kbr	kbr	PROPN
eurjchem-267	160	7	,	,	PUNCT
eurjchem-267	160	8	cm‐1	cm‐1	PROPN
eurjchem-267	160	9	):	):	PUNCT
eurjchem-267	160	10	3310	3310	NUM
eurjchem-267	160	11	ν(nh	ν(nh	NOUN
eurjchem-267	160	12	)	)	PUNCT
eurjchem-267	160	13	,	,	PUNCT
eurjchem-267	160	14	1668	1668	NUM
eurjchem-267	160	15	ν(c	ν(c	NOUN
eurjchem-267	160	16	=	=	PUNCT
eurjchem-267	160	17	oamide	oamide	ADV
eurjchem-267	160	18	)	)	PUNCT
eurjchem-267	160	19	,	,	PUNCT
eurjchem-267	160	20	1622	1622	NUM
eurjchem-267	160	21	ν(c	ν(c	NOUN
eurjchem-267	160	22	=	=	SYM
eurjchem-267	160	23	n	n	NUM
eurjchem-267	160	24	)	)	PUNCT
eurjchem-267	160	25	,	,	PUNCT
eurjchem-267	160	26	1606	1606	NUM
eurjchem-267	160	27	ν(c	ν(c	PROPN
eurjchem-267	160	28	=	=	SYM
eurjchem-267	160	29	c	c	NOUN
eurjchem-267	160	30	)	)	PUNCT
eurjchem-267	160	31	.	.	PUNCT
eurjchem-267	161	1	1h	1h	NUM
eurjchem-267	161	2	nmr	nmr	NOUN
eurjchem-267	161	3	(	(	PUNCT
eurjchem-267	161	4	200	200	NUM
eurjchem-267	161	5	mhz	mhz	NOUN
eurjchem-267	161	6	,	,	PUNCT
eurjchem-267	161	7	dmso‐d6	dmso‐d6	NUM
eurjchem-267	161	8	):	):	PUNCT
eurjchem-267	161	9	8.9	8.9	NUM
eurjchem-267	161	10	(	(	PUNCT
eurjchem-267	161	11	br.s	br.s	PROPN
eurjchem-267	161	12	,	,	PUNCT
eurjchem-267	161	13	1h	1h	NUM
eurjchem-267	161	14	,	,	PUNCT
eurjchem-267	161	15	exchangeable	exchangeable	ADJ
eurjchem-267	161	16	with	with	ADP
eurjchem-267	161	17	d2o	d2o	NOUN
eurjchem-267	161	18	)	)	PUNCT
eurjchem-267	161	19	,	,	PUNCT
eurjchem-267	161	20	8.4‐6.8	8.4‐6.8	NUM
eurjchem-267	161	21	(	(	PUNCT
eurjchem-267	161	22	m	m	PROPN
eurjchem-267	161	23	,	,	PUNCT
eurjchem-267	161	24	21harom	21harom	NUM
eurjchem-267	161	25	.	.	PUNCT
eurjchem-267	162	1	+	+	CCONJ
eurjchem-267	162	2	olefinic	olefinic	ADJ
eurjchem-267	162	3	protons	proton	NOUN
eurjchem-267	162	4	)	)	PUNCT
eurjchem-267	162	5	.	.	PUNCT
eurjchem-267	163	1	ms	ms	NOUN
eurjchem-267	163	2	(	(	PUNCT
eurjchem-267	163	3	ei	ei	PROPN
eurjchem-267	163	4	,	,	PUNCT
eurjchem-267	163	5	m	m	PROPN
eurjchem-267	163	6	/	/	SYM
eurjchem-267	163	7	z	z	PROPN
eurjchem-267	163	8	(	(	PUNCT
eurjchem-267	163	9	%	%	NOUN
eurjchem-267	163	10	)	)	PUNCT
eurjchem-267	163	11	):	):	PUNCT
eurjchem-267	163	12	466	466	NUM
eurjchem-267	163	13	(	(	PUNCT
eurjchem-267	163	14	m+	m+	NUM
eurjchem-267	163	15	.	.	PROPN
eurjchem-267	163	16	,	,	PUNCT
eurjchem-267	163	17	3.9	3.9	NUM
eurjchem-267	163	18	)	)	PUNCT
eurjchem-267	163	19	,	,	PUNCT
eurjchem-267	163	20	365	365	NUM
eurjchem-267	163	21	(	(	PUNCT
eurjchem-267	163	22	16.9	16.9	NUM
eurjchem-267	163	23	)	)	PUNCT
eurjchem-267	163	24	,	,	PUNCT
eurjchem-267	163	25	350	350	NUM
eurjchem-267	163	26	(	(	PUNCT
eurjchem-267	163	27	13.6	13.6	NUM
eurjchem-267	163	28	)	)	PUNCT
eurjchem-267	163	29	,	,	PUNCT
eurjchem-267	163	30	261	261	NUM
eurjchem-267	163	31	(	(	PUNCT
eurjchem-267	163	32	17.6	17.6	NUM
eurjchem-267	163	33	)	)	PUNCT
eurjchem-267	163	34	,	,	PUNCT
eurjchem-267	163	35	105	105	NUM
eurjchem-267	163	36	(	(	PUNCT
eurjchem-267	163	37	100	100	NUM
eurjchem-267	163	38	)	)	PUNCT
eurjchem-267	163	39	,	,	PUNCT
eurjchem-267	163	40	77	77	NUM
eurjchem-267	163	41	(	(	PUNCT
eurjchem-267	163	42	81.6	81.6	NUM
eurjchem-267	163	43	)	)	PUNCT
eurjchem-267	163	44	.	.	PUNCT
eurjchem-267	164	1	anal	anal	PROPN
eurjchem-267	164	2	.	.	PUNCT
eurjchem-267	164	3	calcd	calcd	NOUN
eurjchem-267	164	4	.	.	PUNCT
eurjchem-267	165	1	for	for	ADP
eurjchem-267	165	2	c31h22n4o	c31h22n4o	NOUN
eurjchem-267	165	3	(	(	PUNCT
eurjchem-267	165	4	466	466	NUM
eurjchem-267	165	5	):	):	PUNCT
eurjchem-267	165	6	c	c	X
eurjchem-267	165	7	,	,	PUNCT
eurjchem-267	165	8	79.83;	79.83;	PROPN
eurjchem-267	165	9	h	h	NOUN
eurjchem-267	165	10	,	,	PUNCT
eurjchem-267	165	11	4.72	4.72	NUM
eurjchem-267	165	12	;	;	PUNCT
eurjchem-267	165	13	n	n	CCONJ
eurjchem-267	165	14	,	,	PUNCT
eurjchem-267	165	15	12.02	12.02	NUM
eurjchem-267	165	16	.	.	PUNCT
eurjchem-267	166	1	found	find	VERB
eurjchem-267	166	2	:	:	PUNCT
eurjchem-267	167	1	c	c	X
eurjchem-267	167	2	,	,	PUNCT
eurjchem-267	167	3	79.66	79.66	NUM
eurjchem-267	167	4	;	;	PUNCT
eurjchem-267	167	5	h	h	X
eurjchem-267	167	6	,	,	PUNCT
eurjchem-267	167	7	4.64	4.64	NUM
eurjchem-267	167	8	;	;	PUNCT
eurjchem-267	167	9	n	n	CCONJ
eurjchem-267	167	10	,	,	PUNCT
eurjchem-267	167	11	12.21	12.21	NUM
eurjchem-267	167	12	%	%	NOUN
eurjchem-267	167	13	.	.	PUNCT
eurjchem-267	168	1	408	408	NUM
eurjchem-267	168	2	mahmoud	mahmoud	PROPN
eurjchem-267	168	3	et	et	PROPN
eurjchem-267	168	4	al	al	PROPN
eurjchem-267	168	5	.	.	PUNCT
eurjchem-267	168	6	/	/	SYM
eurjchem-267	168	7	european	european	PROPN
eurjchem-267	168	8	journal	journal	PROPN
eurjchem-267	168	9	of	of	ADP
eurjchem-267	168	10	chemistry	chemistry	NOUN
eurjchem-267	168	11	2	2	NUM
eurjchem-267	168	12	(	(	PUNCT
eurjchem-267	168	13	3	3	NUM
eurjchem-267	168	14	)	)	PUNCT
eurjchem-267	168	15	(	(	PUNCT
eurjchem-267	168	16	2011	2011	NUM
eurjchem-267	168	17	)	)	PUNCT
eurjchem-267	168	18	404‐409	404‐409	NUM
eurjchem-267	168	19	2.13	2.13	NUM
eurjchem-267	168	20	.	.	PUNCT
eurjchem-267	169	1	quinazolin‐4(h)‐one	quinazolin‐4(h)‐one	PRON
eurjchem-267	169	2	derivative	derivative	ADJ
eurjchem-267	169	3	(	(	PUNCT
eurjchem-267	169	4	12	12	NUM
eurjchem-267	169	5	)	)	PUNCT
eurjchem-267	169	6	to	to	ADP
eurjchem-267	169	7	a	a	DET
eurjchem-267	169	8	solution	solution	NOUN
eurjchem-267	169	9	of	of	ADP
eurjchem-267	169	10	1	1	NUM
eurjchem-267	169	11	(	(	PUNCT
eurjchem-267	169	12	0.01	0.01	NUM
eurjchem-267	169	13	mol	mol	NOUN
eurjchem-267	169	14	)	)	PUNCT
eurjchem-267	169	15	in	in	ADP
eurjchem-267	169	16	pyridine	pyridine	NOUN
eurjchem-267	169	17	(	(	PUNCT
eurjchem-267	169	18	30	30	NUM
eurjchem-267	169	19	ml	ml	NOUN
eurjchem-267	169	20	)	)	PUNCT
eurjchem-267	169	21	,	,	PUNCT
eurjchem-267	169	22	n‐(1‐	n‐(1‐	PROPN
eurjchem-267	169	23	naphthyl)ethane‐1,2‐diamine	naphthyl)ethane‐1,2‐diamine	PRON
eurjchem-267	169	24	hydrochloride	hydrochloride	NOUN
eurjchem-267	169	25	(	(	PUNCT
eurjchem-267	169	26	3.3	3.3	NUM
eurjchem-267	169	27	g	g	NOUN
eurjchem-267	169	28	,	,	PUNCT
eurjchem-267	169	29	0.015	0.015	NUM
eurjchem-267	169	30	mol	mol	NOUN
eurjchem-267	169	31	)	)	PUNCT
eurjchem-267	169	32	was	be	AUX
eurjchem-267	169	33	added	add	VERB
eurjchem-267	169	34	and	and	CCONJ
eurjchem-267	169	35	the	the	DET
eurjchem-267	169	36	reaction	reaction	NOUN
eurjchem-267	169	37	mixture	mixture	NOUN
eurjchem-267	169	38	was	be	AUX
eurjchem-267	169	39	heated	heat	VERB
eurjchem-267	169	40	under	under	ADP
eurjchem-267	169	41	reflux	reflux	NOUN
eurjchem-267	169	42	for	for	ADP
eurjchem-267	169	43	10	10	NUM
eurjchem-267	169	44	hrs	hrs	NOUN
eurjchem-267	169	45	(	(	PUNCT
eurjchem-267	169	46	tlc	tlc	NOUN
eurjchem-267	169	47	)	)	PUNCT
eurjchem-267	169	48	.	.	PUNCT
eurjchem-267	170	1	the	the	DET
eurjchem-267	170	2	cooled	cool	VERB
eurjchem-267	170	3	reaction	reaction	NOUN
eurjchem-267	170	4	mixture	mixture	NOUN
eurjchem-267	170	5	was	be	AUX
eurjchem-267	170	6	acidified	acidify	VERB
eurjchem-267	170	7	with	with	ADP
eurjchem-267	170	8	cold	cold	ADJ
eurjchem-267	170	9	dilute	dilute	NOUN
eurjchem-267	170	10	hydrochloric	hydrochloric	ADJ
eurjchem-267	170	11	acid	acid	NOUN
eurjchem-267	170	12	.	.	PUNCT
eurjchem-267	171	1	the	the	DET
eurjchem-267	171	2	solid	solid	ADJ
eurjchem-267	171	3	deposited	deposit	VERB
eurjchem-267	171	4	was	be	AUX
eurjchem-267	171	5	filtered	filter	VERB
eurjchem-267	171	6	off	off	ADP
eurjchem-267	171	7	,	,	PUNCT
eurjchem-267	171	8	dried	dry	VERB
eurjchem-267	171	9	and	and	CCONJ
eurjchem-267	171	10	recrystallized	recrystallize	VERB
eurjchem-267	171	11	from	from	ADP
eurjchem-267	171	12	toluene	toluene	NOUN
eurjchem-267	171	13	to	to	PART
eurjchem-267	171	14	give	give	VERB
eurjchem-267	171	15	12	12	NUM
eurjchem-267	171	16	as	as	ADP
eurjchem-267	171	17	pale	pale	ADJ
eurjchem-267	171	18	yellow	yellow	ADJ
eurjchem-267	171	19	crystals	crystal	NOUN
eurjchem-267	171	20	(	(	PUNCT
eurjchem-267	171	21	scheme	scheme	NOUN
eurjchem-267	171	22	3	3	NUM
eurjchem-267	171	23	)	)	PUNCT
eurjchem-267	171	24	.	.	PUNCT
eurjchem-267	172	1	yield	yield	NOUN
eurjchem-267	172	2	:	:	PUNCT
eurjchem-267	172	3	83	83	NUM
eurjchem-267	172	4	%	%	NOUN
eurjchem-267	172	5	.	.	PUNCT
eurjchem-267	173	1	m.p	m.p	PROPN
eurjchem-267	173	2	.	.	PROPN
eurjchem-267	173	3	:	:	PUNCT
eurjchem-267	174	1	200‐202	200‐202	PROPN
eurjchem-267	174	2	oc	oc	PROPN
eurjchem-267	174	3	.	.	PROPN
eurjchem-267	174	4	ir	ir	PROPN
eurjchem-267	174	5	(	(	PUNCT
eurjchem-267	174	6	kbr	kbr	PROPN
eurjchem-267	174	7	,	,	PUNCT
eurjchem-267	174	8	cm‐1	cm‐1	PROPN
eurjchem-267	174	9	):	):	PUNCT
eurjchem-267	174	10	br	br	PROPN
eurjchem-267	174	11	.	.	PROPN
eurjchem-267	174	12	3420	3420	NUM
eurjchem-267	174	13	,	,	PUNCT
eurjchem-267	174	14	3302	3302	NUM
eurjchem-267	174	15	ν(nh	ν(nh	NOUN
eurjchem-267	174	16	)	)	PUNCT
eurjchem-267	174	17	,	,	PUNCT
eurjchem-267	174	18	1738	1738	NUM
eurjchem-267	174	19	ν(c	ν(c	PROPN
eurjchem-267	174	20	=	=	SYM
eurjchem-267	174	21	o	o	NOUN
eurjchem-267	174	22	)	)	PUNCT
eurjchem-267	174	23	,	,	PUNCT
eurjchem-267	174	24	1668	1668	NUM
eurjchem-267	174	25	ν(c	ν(c	NOUN
eurjchem-267	174	26	=	=	SYM
eurjchem-267	174	27	o	o	NOUN
eurjchem-267	174	28	)	)	PUNCT
eurjchem-267	174	29	,	,	PUNCT
eurjchem-267	174	30	1600	1600	NUM
eurjchem-267	174	31	ν(c	ν(c	PROPN
eurjchem-267	174	32	=	=	SYM
eurjchem-267	174	33	c	c	NOUN
eurjchem-267	174	34	)	)	PUNCT
eurjchem-267	174	35	.	.	PUNCT
eurjchem-267	175	1	1h	1h	NUM
eurjchem-267	175	2	nmr	nmr	NOUN
eurjchem-267	175	3	(	(	PUNCT
eurjchem-267	175	4	200	200	NUM
eurjchem-267	175	5	mhz	mhz	NOUN
eurjchem-267	175	6	,	,	PUNCT
eurjchem-267	175	7	dmso‐d6	dmso‐d6	NUM
eurjchem-267	175	8	):	):	PUNCT
eurjchem-267	175	9	8.9	8.9	NUM
eurjchem-267	175	10	(	(	PUNCT
eurjchem-267	175	11	br.s	br.s	PROPN
eurjchem-267	175	12	,	,	PUNCT
eurjchem-267	175	13	1h	1h	NUM
eurjchem-267	175	14	,	,	PUNCT
eurjchem-267	175	15	exchangeable	exchangeable	ADJ
eurjchem-267	175	16	with	with	ADP
eurjchem-267	175	17	d2o	d2o	NOUN
eurjchem-267	175	18	)	)	PUNCT
eurjchem-267	175	19	,	,	PUNCT
eurjchem-267	175	20	8.4‐7.1	8.4‐7.1	NUM
eurjchem-267	175	21	(	(	PUNCT
eurjchem-267	175	22	m	m	PROPN
eurjchem-267	175	23	,	,	PUNCT
eurjchem-267	175	24	21harom	21harom	NUM
eurjchem-267	175	25	.	.	PUNCT
eurjchem-267	175	26	)	)	PUNCT
eurjchem-267	175	27	,	,	PUNCT
eurjchem-267	175	28	7.0‐6.1	7.0‐6.1	NUM
eurjchem-267	175	29	(	(	PUNCT
eurjchem-267	175	30	m	m	PROPN
eurjchem-267	175	31	,	,	PUNCT
eurjchem-267	175	32	3h	3h	NUM
eurjchem-267	175	33	)	)	PUNCT
eurjchem-267	175	34	,	,	PUNCT
eurjchem-267	175	35	3.6	3.6	NUM
eurjchem-267	175	36	(	(	PUNCT
eurjchem-267	175	37	m	m	PROPN
eurjchem-267	175	38	,	,	PUNCT
eurjchem-267	175	39	2h	2h	NUM
eurjchem-267	175	40	)	)	PUNCT
eurjchem-267	175	41	,	,	PUNCT
eurjchem-267	175	42	3.4	3.4	NUM
eurjchem-267	175	43	(	(	PUNCT
eurjchem-267	175	44	t	t	PROPN
eurjchem-267	175	45	,	,	PUNCT
eurjchem-267	175	46	2h	2h	NUM
eurjchem-267	175	47	,	,	PUNCT
eurjchem-267	175	48	j	j	PROPN
eurjchem-267	175	49	=	=	SYM
eurjchem-267	175	50	4.6	4.6	NUM
eurjchem-267	175	51	hz	hz	NOUN
eurjchem-267	175	52	)	)	PUNCT
eurjchem-267	175	53	.	.	PUNCT
eurjchem-267	176	1	ms	ms	NOUN
eurjchem-267	176	2	(	(	PUNCT
eurjchem-267	176	3	ei	ei	PROPN
eurjchem-267	176	4	,	,	PUNCT
eurjchem-267	176	5	m	m	PROPN
eurjchem-267	176	6	/	/	SYM
eurjchem-267	176	7	z	z	PROPN
eurjchem-267	176	8	(	(	PUNCT
eurjchem-267	176	9	%	%	NOUN
eurjchem-267	176	10	)	)	PUNCT
eurjchem-267	176	11	):	):	PUNCT
eurjchem-267	176	12	435	435	NUM
eurjchem-267	176	13	(	(	PUNCT
eurjchem-267	176	14	m+	m+	NUM
eurjchem-267	176	15	.	.	PUNCT
eurjchem-267	176	16	–	–	PUNCT
eurjchem-267	176	17	c10h7	c10h7	NOUN
eurjchem-267	176	18	,	,	PUNCT
eurjchem-267	176	19	12.7	12.7	NUM
eurjchem-267	176	20	)	)	PUNCT
eurjchem-267	176	21	,	,	PUNCT
eurjchem-267	176	22	393	393	NUM
eurjchem-267	176	23	(	(	PUNCT
eurjchem-267	176	24	70.2	70.2	NUM
eurjchem-267	176	25	)	)	PUNCT
eurjchem-267	176	26	,	,	PUNCT
eurjchem-267	176	27	145	145	NUM
eurjchem-267	176	28	(	(	PUNCT
eurjchem-267	176	29	17.8	17.8	NUM
eurjchem-267	176	30	)	)	PUNCT
eurjchem-267	176	31	,	,	PUNCT
eurjchem-267	176	32	105	105	NUM
eurjchem-267	176	33	(	(	PUNCT
eurjchem-267	176	34	100	100	NUM
eurjchem-267	176	35	)	)	PUNCT
eurjchem-267	176	36	,	,	PUNCT
eurjchem-267	176	37	77	77	NUM
eurjchem-267	176	38	(	(	PUNCT
eurjchem-267	176	39	76.8	76.8	NUM
eurjchem-267	176	40	)	)	PUNCT
eurjchem-267	176	41	.	.	PUNCT
eurjchem-267	177	1	anal	anal	PROPN
eurjchem-267	177	2	.	.	PUNCT
eurjchem-267	177	3	calcd	calcd	NOUN
eurjchem-267	177	4	.	.	PUNCT
eurjchem-267	178	1	for	for	ADP
eurjchem-267	178	2	c37h30n4o2	c37h30n4o2	PROPN
eurjchem-267	178	3	(	(	PUNCT
eurjchem-267	178	4	562	562	NUM
eurjchem-267	178	5	):	):	PUNCT
eurjchem-267	178	6	c	c	X
eurjchem-267	178	7	,	,	PUNCT
eurjchem-267	178	8	79.0;	79.0;	NUM
eurjchem-267	178	9	h	h	NOUN
eurjchem-267	178	10	,	,	PUNCT
eurjchem-267	178	11	5.34	5.34	NUM
eurjchem-267	178	12	;	;	PUNCT
eurjchem-267	178	13	n	n	CCONJ
eurjchem-267	178	14	,	,	PUNCT
eurjchem-267	178	15	9.96	9.96	NUM
eurjchem-267	178	16	.	.	PUNCT
eurjchem-267	178	17	found	find	VERB
eurjchem-267	178	18	:	:	PUNCT
eurjchem-267	179	1	c	c	X
eurjchem-267	179	2	,	,	PUNCT
eurjchem-267	179	3	79.13	79.13	NUM
eurjchem-267	179	4	;	;	PUNCT
eurjchem-267	179	5	h	h	NOUN
eurjchem-267	179	6	,	,	PUNCT
eurjchem-267	179	7	5.0	5.0	NUM
eurjchem-267	179	8	;	;	PUNCT
eurjchem-267	179	9	n	n	CCONJ
eurjchem-267	179	10	,	,	PUNCT
eurjchem-267	179	11	9.66	9.66	NUM
eurjchem-267	179	12	%	%	NOUN
eurjchem-267	179	13	.	.	PUNCT
eurjchem-267	180	1	2.14	2.14	NUM
eurjchem-267	180	2	.	.	PUNCT
eurjchem-267	181	1	3‐(pyrimidin‐2‐yl)‐2‐[(1z,3e)‐1‐benzamido‐4‐phenyl‐	3‐(pyrimidin‐2‐yl)‐2‐[(1z,3e)‐1‐benzamido‐4‐phenyl‐	NUM
eurjchem-267	181	2	1,3‐butadien‐1‐yl]quinazolin‐4(h)‐one	1,3‐butadien‐1‐yl]quinazolin‐4(h)‐one	NOUN
eurjchem-267	181	3	(	(	PUNCT
eurjchem-267	181	4	13	13	NUM
eurjchem-267	181	5	)	)	PUNCT
eurjchem-267	181	6	a	a	DET
eurjchem-267	181	7	mixture	mixture	NOUN
eurjchem-267	181	8	of	of	ADP
eurjchem-267	181	9	1	1	NUM
eurjchem-267	181	10	(	(	PUNCT
eurjchem-267	181	11	0.01	0.01	NUM
eurjchem-267	181	12	mol	mol	NOUN
eurjchem-267	181	13	)	)	PUNCT
eurjchem-267	181	14	and	and	CCONJ
eurjchem-267	181	15	2‐aminopyrimidine	2‐aminopyrimidine	NUM
eurjchem-267	181	16	(	(	PUNCT
eurjchem-267	181	17	1.4	1.4	NUM
eurjchem-267	181	18	g	g	NOUN
eurjchem-267	181	19	,	,	PUNCT
eurjchem-267	181	20	0.015	0.015	NUM
eurjchem-267	181	21	mol	mol	NOUN
eurjchem-267	181	22	)	)	PUNCT
eurjchem-267	181	23	was	be	AUX
eurjchem-267	181	24	heated	heat	VERB
eurjchem-267	181	25	with	with	ADP
eurjchem-267	181	26	stirring	stir	VERB
eurjchem-267	181	27	on	on	ADP
eurjchem-267	181	28	an	an	DET
eurjchem-267	181	29	oil‐bath	oil‐bath	NOUN
eurjchem-267	181	30	for	for	ADP
eurjchem-267	181	31	4	4	NUM
eurjchem-267	181	32	hrs	hrs	NOUN
eurjchem-267	181	33	at	at	ADP
eurjchem-267	181	34	200	200	NUM
eurjchem-267	181	35	oc	oc	NOUN
eurjchem-267	181	36	.	.	PUNCT
eurjchem-267	182	1	the	the	DET
eurjchem-267	182	2	reaction	reaction	NOUN
eurjchem-267	182	3	mixture	mixture	NOUN
eurjchem-267	182	4	was	be	AUX
eurjchem-267	182	5	triturated	triturate	VERB
eurjchem-267	182	6	with	with	ADP
eurjchem-267	182	7	dilute	dilute	NOUN
eurjchem-267	182	8	methanol	methanol	NOUN
eurjchem-267	182	9	and	and	CCONJ
eurjchem-267	182	10	the	the	DET
eurjchem-267	182	11	separated	separate	VERB
eurjchem-267	182	12	solid	solid	ADJ
eurjchem-267	182	13	was	be	AUX
eurjchem-267	182	14	filtered	filter	VERB
eurjchem-267	182	15	off	off	ADP
eurjchem-267	182	16	,	,	PUNCT
eurjchem-267	182	17	washed	wash	VERB
eurjchem-267	182	18	several	several	ADJ
eurjchem-267	182	19	times	time	NOUN
eurjchem-267	182	20	with	with	ADP
eurjchem-267	182	21	diethyl	diethyl	NOUN
eurjchem-267	182	22	ether	ether	NOUN
eurjchem-267	182	23	,	,	PUNCT
eurjchem-267	182	24	dried	dry	VERB
eurjchem-267	182	25	and	and	CCONJ
eurjchem-267	182	26	recrystallized	recrystallize	VERB
eurjchem-267	182	27	from	from	ADP
eurjchem-267	182	28	ethanol	ethanol	NOUN
eurjchem-267	182	29	to	to	PART
eurjchem-267	182	30	give	give	VERB
eurjchem-267	182	31	13	13	NUM
eurjchem-267	182	32	as	as	ADP
eurjchem-267	182	33	a	a	DET
eurjchem-267	182	34	light	light	ADJ
eurjchem-267	182	35	brown	brown	ADJ
eurjchem-267	182	36	crystals	crystal	NOUN
eurjchem-267	182	37	(	(	PUNCT
eurjchem-267	182	38	scheme	scheme	NOUN
eurjchem-267	182	39	3	3	NUM
eurjchem-267	182	40	)	)	PUNCT
eurjchem-267	182	41	.	.	PUNCT
eurjchem-267	183	1	yield	yield	NOUN
eurjchem-267	183	2	:	:	PUNCT
eurjchem-267	183	3	68	68	NUM
eurjchem-267	183	4	%	%	NOUN
eurjchem-267	183	5	.	.	PUNCT
eurjchem-267	184	1	m.p	m.p	PROPN
eurjchem-267	184	2	.	.	PROPN
eurjchem-267	184	3	:	:	PUNCT
eurjchem-267	185	1	166‐167	166‐167	NUM
eurjchem-267	185	2	oc	oc	NOUN
eurjchem-267	185	3	.	.	PUNCT
eurjchem-267	185	4	ir	ir	PROPN
eurjchem-267	185	5	(	(	PUNCT
eurjchem-267	185	6	kbr	kbr	PROPN
eurjchem-267	185	7	,	,	PUNCT
eurjchem-267	185	8	cm‐1	cm‐1	PROPN
eurjchem-267	185	9	):	):	PUNCT
eurjchem-267	185	10	3264	3264	NUM
eurjchem-267	185	11	ν(nh	ν(nh	NOUN
eurjchem-267	185	12	)	)	PUNCT
eurjchem-267	185	13	,	,	PUNCT
eurjchem-267	185	14	1711	1711	NUM
eurjchem-267	185	15	,	,	PUNCT
eurjchem-267	185	16	1672	1672	NUM
eurjchem-267	185	17	ν(c	ν(c	NOUN
eurjchem-267	185	18	=	=	SYM
eurjchem-267	185	19	o	o	NOUN
eurjchem-267	185	20	)	)	PUNCT
eurjchem-267	185	21	,	,	PUNCT
eurjchem-267	185	22	1638	1638	NUM
eurjchem-267	185	23	ν(c	ν(c	NOUN
eurjchem-267	185	24	=	=	SYM
eurjchem-267	185	25	n	n	NUM
eurjchem-267	185	26	)	)	PUNCT
eurjchem-267	185	27	,	,	PUNCT
eurjchem-267	185	28	1608	1608	NUM
eurjchem-267	185	29	ν(c	ν(c	PROPN
eurjchem-267	185	30	=	=	SYM
eurjchem-267	185	31	c	c	NOUN
eurjchem-267	185	32	)	)	PUNCT
eurjchem-267	185	33	.	.	PUNCT
eurjchem-267	186	1	1h	1h	NUM
eurjchem-267	186	2	nmr	nmr	NOUN
eurjchem-267	186	3	(	(	PUNCT
eurjchem-267	186	4	200	200	NUM
eurjchem-267	186	5	mhz	mhz	NOUN
eurjchem-267	186	6	,	,	PUNCT
eurjchem-267	186	7	cdcl3	cdcl3	NOUN
eurjchem-267	186	8	):	):	PUNCT
eurjchem-267	186	9	9.0	9.0	NUM
eurjchem-267	186	10	(	(	PUNCT
eurjchem-267	186	11	s	s	PROPN
eurjchem-267	186	12	,	,	PUNCT
eurjchem-267	186	13	1h	1h	NUM
eurjchem-267	186	14	,	,	PUNCT
eurjchem-267	186	15	exchangeable	exchangeable	ADJ
eurjchem-267	186	16	with	with	ADP
eurjchem-267	186	17	d2o	d2o	NOUN
eurjchem-267	186	18	)	)	PUNCT
eurjchem-267	186	19	,	,	PUNCT
eurjchem-267	186	20	8.7‐7.12	8.7‐7.12	NUM
eurjchem-267	186	21	(	(	PUNCT
eurjchem-267	186	22	m	m	PROPN
eurjchem-267	186	23	,	,	PUNCT
eurjchem-267	186	24	17harom	17harom	NUM
eurjchem-267	186	25	.	.	PUNCT
eurjchem-267	186	26	)	)	PUNCT
eurjchem-267	186	27	,	,	PUNCT
eurjchem-267	186	28	6.8‐	6.8‐	NUM
eurjchem-267	186	29	6.5	6.5	NUM
eurjchem-267	186	30	(	(	PUNCT
eurjchem-267	186	31	m	m	PROPN
eurjchem-267	186	32	,	,	PUNCT
eurjchem-267	186	33	3h	3h	NUM
eurjchem-267	186	34	)	)	PUNCT
eurjchem-267	186	35	.	.	PUNCT
eurjchem-267	187	1	ms	ms	NOUN
eurjchem-267	187	2	(	(	PUNCT
eurjchem-267	187	3	ei	ei	PROPN
eurjchem-267	187	4	,	,	PUNCT
eurjchem-267	187	5	m	m	PROPN
eurjchem-267	187	6	/	/	SYM
eurjchem-267	187	7	z	z	PROPN
eurjchem-267	187	8	(	(	PUNCT
eurjchem-267	187	9	%	%	NOUN
eurjchem-267	187	10	)	)	PUNCT
eurjchem-267	187	11	):	):	PUNCT
eurjchem-267	187	12	472	472	NUM
eurjchem-267	187	13	(	(	PUNCT
eurjchem-267	187	14	m+.+1	m+.+1	NOUN
eurjchem-267	187	15	,	,	PUNCT
eurjchem-267	187	16	20.2	20.2	NUM
eurjchem-267	187	17	)	)	PUNCT
eurjchem-267	187	18	,	,	PUNCT
eurjchem-267	187	19	393	393	NUM
eurjchem-267	187	20	(	(	PUNCT
eurjchem-267	187	21	66.1	66.1	NUM
eurjchem-267	187	22	)	)	PUNCT
eurjchem-267	187	23	,	,	PUNCT
eurjchem-267	187	24	105	105	NUM
eurjchem-267	187	25	(	(	PUNCT
eurjchem-267	187	26	100	100	NUM
eurjchem-267	187	27	)	)	PUNCT
eurjchem-267	187	28	,	,	PUNCT
eurjchem-267	187	29	77	77	NUM
eurjchem-267	187	30	(	(	PUNCT
eurjchem-267	187	31	60.1	60.1	NUM
eurjchem-267	187	32	)	)	PUNCT
eurjchem-267	187	33	.	.	PUNCT
eurjchem-267	188	1	anal	anal	PROPN
eurjchem-267	188	2	.	.	PUNCT
eurjchem-267	188	3	calcd	calcd	NOUN
eurjchem-267	188	4	.	.	PUNCT
eurjchem-267	189	1	for	for	ADP
eurjchem-267	189	2	c29h21n5o2	c29h21n5o2	PROPN
eurjchem-267	189	3	(	(	PUNCT
eurjchem-267	189	4	471	471	NUM
eurjchem-267	189	5	):	):	PUNCT
eurjchem-267	189	6	c	c	X
eurjchem-267	189	7	,	,	PUNCT
eurjchem-267	189	8	73.88;	73.88;	NUM
eurjchem-267	189	9	h	h	NOUN
eurjchem-267	189	10	,	,	PUNCT
eurjchem-267	189	11	4.45	4.45	NUM
eurjchem-267	189	12	;	;	PUNCT
eurjchem-267	189	13	n	n	CCONJ
eurjchem-267	189	14	,	,	PUNCT
eurjchem-267	189	15	14.86	14.86	NUM
eurjchem-267	189	16	.	.	PUNCT
eurjchem-267	189	17	found	find	VERB
eurjchem-267	189	18	:	:	PUNCT
eurjchem-267	190	1	c	c	X
eurjchem-267	190	2	,	,	PUNCT
eurjchem-267	190	3	73.62	73.62	NUM
eurjchem-267	190	4	;	;	PUNCT
eurjchem-267	190	5	h	h	NOUN
eurjchem-267	190	6	,	,	PUNCT
eurjchem-267	190	7	4.37	4.37	NUM
eurjchem-267	190	8	;	;	PUNCT
eurjchem-267	190	9	n	n	CCONJ
eurjchem-267	190	10	,	,	PUNCT
eurjchem-267	190	11	14.58	14.58	NUM
eurjchem-267	190	12	%	%	NOUN
eurjchem-267	190	13	.	.	PUNCT
eurjchem-267	191	1	3	3	X
eurjchem-267	191	2	.	.	NOUN
eurjchem-267	191	3	results	result	NOUN
eurjchem-267	191	4	and	and	CCONJ
eurjchem-267	191	5	discussion	discussion	NOUN
eurjchem-267	191	6	benzoxazinones	benzoxazinone	NOUN
eurjchem-267	191	7	can	can	AUX
eurjchem-267	191	8	be	be	AUX
eurjchem-267	191	9	considered	consider	VERB
eurjchem-267	191	10	as	as	ADP
eurjchem-267	191	11	semi	semi	ADV
eurjchem-267	191	12	acid	acid	NOUN
eurjchem-267	191	13	anhydride	anhydride	NOUN
eurjchem-267	191	14	and	and	CCONJ
eurjchem-267	191	15	they	they	PRON
eurjchem-267	191	16	undergo	undergo	VERB
eurjchem-267	191	17	many	many	ADJ
eurjchem-267	191	18	reactions	reaction	NOUN
eurjchem-267	191	19	of	of	ADP
eurjchem-267	191	20	true	true	ADJ
eurjchem-267	191	21	acid	acid	NOUN
eurjchem-267	191	22	anhydrides	anhydride	NOUN
eurjchem-267	192	1	[	[	X
eurjchem-267	192	2	35,36	35,36	NUM
eurjchem-267	192	3	]	]	PUNCT
eurjchem-267	192	4	.	.	PUNCT
eurjchem-267	193	1	acid	acid	PROPN
eurjchem-267	193	2	anhydrides	anhydride	NOUN
eurjchem-267	193	3	react	react	VERB
eurjchem-267	193	4	with	with	ADP
eurjchem-267	193	5	schiff	schiff	PROPN
eurjchem-267	193	6	’s	’s	PART
eurjchem-267	193	7	bases	basis	NOUN
eurjchem-267	193	8	and	and	CCONJ
eurjchem-267	193	9	azines	azine	NOUN
eurjchem-267	193	10	to	to	PART
eurjchem-267	193	11	give	give	VERB
eurjchem-267	193	12	products	product	NOUN
eurjchem-267	193	13	depending	depend	VERB
eurjchem-267	193	14	upon	upon	SCONJ
eurjchem-267	193	15	reaction	reaction	NOUN
eurjchem-267	193	16	conditions	condition	NOUN
eurjchem-267	193	17	.	.	PUNCT
eurjchem-267	194	1	the	the	DET
eurjchem-267	194	2	reaction	reaction	NOUN
eurjchem-267	194	3	in	in	ADP
eurjchem-267	194	4	many	many	ADJ
eurjchem-267	194	5	cases	case	NOUN
eurjchem-267	194	6	involved	involve	VERB
eurjchem-267	194	7	the	the	DET
eurjchem-267	194	8	displacement	displacement	NOUN
eurjchem-267	194	9	of	of	ADP
eurjchem-267	194	10	arylidene	arylidene	NOUN
eurjchem-267	194	11	group	group	NOUN
eurjchem-267	194	12	of	of	ADP
eurjchem-267	194	13	the	the	DET
eurjchem-267	194	14	imine	imine	ADJ
eurjchem-267	194	15	molecule	molecule	NOUN
eurjchem-267	194	16	.	.	PUNCT
eurjchem-267	195	1	the	the	DET
eurjchem-267	195	2	present	present	ADJ
eurjchem-267	195	3	investigation	investigation	NOUN
eurjchem-267	195	4	was	be	AUX
eurjchem-267	195	5	to	to	PART
eurjchem-267	195	6	involve	involve	VERB
eurjchem-267	195	7	the	the	DET
eurjchem-267	195	8	reaction	reaction	NOUN
eurjchem-267	195	9	of	of	ADP
eurjchem-267	195	10	compound	compound	NOUN
eurjchem-267	195	11	1	1	NUM
eurjchem-267	195	12	with	with	ADP
eurjchem-267	195	13	schiff	schiff	PROPN
eurjchem-267	195	14	’s	’s	PART
eurjchem-267	195	15	bases	basis	NOUN
eurjchem-267	195	16	and	and	CCONJ
eurjchem-267	195	17	azines	azine	NOUN
eurjchem-267	195	18	.	.	PUNCT
eurjchem-267	196	1	the	the	DET
eurjchem-267	196	2	interaction	interaction	NOUN
eurjchem-267	196	3	of	of	ADP
eurjchem-267	196	4	equimolecular	equimolecular	ADJ
eurjchem-267	196	5	amounts	amount	NOUN
eurjchem-267	196	6	of	of	ADP
eurjchem-267	196	7	1	1	NUM
eurjchem-267	196	8	and	and	CCONJ
eurjchem-267	196	9	4‐	4‐	NUM
eurjchem-267	196	10	chlorobenzylidene‐4‐methylaniline	chlorobenzylidene‐4‐methylaniline	PROPN
eurjchem-267	196	11	in	in	ADP
eurjchem-267	196	12	dry	dry	ADJ
eurjchem-267	196	13	benzene	benzene	NOUN
eurjchem-267	196	14	under	under	ADP
eurjchem-267	196	15	reflux	reflux	NOUN
eurjchem-267	196	16	yielded	yield	VERB
eurjchem-267	196	17	2‐substituted	2‐substitute	VERB
eurjchem-267	196	18	amino‐n‐(4‐methyl‐phenyl)benzamide	amino‐n‐(4‐methyl‐phenyl)benzamide	ADV
eurjchem-267	196	19	(	(	PUNCT
eurjchem-267	196	20	2	2	NUM
eurjchem-267	196	21	)	)	PUNCT
eurjchem-267	196	22	.	.	PUNCT
eurjchem-267	197	1	however	however	ADV
eurjchem-267	197	2	,	,	PUNCT
eurjchem-267	197	3	when	when	SCONJ
eurjchem-267	197	4	the	the	DET
eurjchem-267	197	5	reaction	reaction	NOUN
eurjchem-267	197	6	was	be	AUX
eurjchem-267	197	7	conduced	conduce	VERB
eurjchem-267	197	8	in	in	ADP
eurjchem-267	197	9	glacial	glacial	ADJ
eurjchem-267	197	10	acetic	acetic	ADJ
eurjchem-267	197	11	acid	acid	NOUN
eurjchem-267	197	12	containing	contain	VERB
eurjchem-267	197	13	catalytic	catalytic	ADJ
eurjchem-267	197	14	amount	amount	NOUN
eurjchem-267	197	15	of	of	ADP
eurjchem-267	197	16	anhydrous	anhydrous	ADJ
eurjchem-267	197	17	sodium	sodium	NOUN
eurjchem-267	197	18	acetate	acetate	NOUN
eurjchem-267	197	19	,	,	PUNCT
eurjchem-267	197	20	3‐(4‐methylphenyl)‐2‐substituted	3‐(4‐methylphenyl)‐2‐substitute	VERB
eurjchem-267	197	21	quinazolin‐4(h)‐one	quinazolin‐4(h)‐one	NUM
eurjchem-267	197	22	(	(	PUNCT
eurjchem-267	197	23	3	3	NUM
eurjchem-267	197	24	)	)	PUNCT
eurjchem-267	197	25	was	be	AUX
eurjchem-267	197	26	obtained	obtain	VERB
eurjchem-267	197	27	in	in	ADP
eurjchem-267	197	28	quantitative	quantitative	ADJ
eurjchem-267	197	29	yield	yield	NOUN
eurjchem-267	197	30	.	.	PUNCT
eurjchem-267	198	1	the	the	DET
eurjchem-267	198	2	structures	structure	NOUN
eurjchem-267	198	3	of	of	ADP
eurjchem-267	198	4	2	2	NUM
eurjchem-267	198	5	and	and	CCONJ
eurjchem-267	198	6	3	3	NUM
eurjchem-267	198	7	were	be	AUX
eurjchem-267	198	8	rigidly	rigidly	ADV
eurjchem-267	198	9	established	establish	VERB
eurjchem-267	198	10	beside	beside	ADP
eurjchem-267	198	11	the	the	DET
eurjchem-267	198	12	microanalytical	microanalytical	ADJ
eurjchem-267	198	13	and	and	CCONJ
eurjchem-267	198	14	spectral	spectral	ADJ
eurjchem-267	198	15	data	datum	NOUN
eurjchem-267	198	16	by	by	ADP
eurjchem-267	198	17	identity	identity	NOUN
eurjchem-267	198	18	with	with	ADP
eurjchem-267	198	19	authentic	authentic	ADJ
eurjchem-267	198	20	samples	sample	NOUN
eurjchem-267	198	21	(	(	PUNCT
eurjchem-267	198	22	m.p	m.p	PROPN
eurjchem-267	198	23	,	,	PUNCT
eurjchem-267	198	24	mixed	mixed	ADJ
eurjchem-267	198	25	m.p	m.p	PROPN
eurjchem-267	198	26	,	,	PUNCT
eurjchem-267	198	27	tlc	tlc	NOUN
eurjchem-267	198	28	)	)	PUNCT
eurjchem-267	198	29	prepared	prepare	VERB
eurjchem-267	198	30	from	from	ADP
eurjchem-267	198	31	the	the	DET
eurjchem-267	198	32	reaction	reaction	NOUN
eurjchem-267	198	33	of	of	ADP
eurjchem-267	198	34	1	1	NUM
eurjchem-267	198	35	with	with	ADP
eurjchem-267	198	36	p‐toluidine	p‐toluidine	PUNCT
eurjchem-267	198	37	in	in	ADP
eurjchem-267	198	38	refluxing	refluxing	NOUN
eurjchem-267	198	39	ethanol	ethanol	NOUN
eurjchem-267	198	40	or	or	CCONJ
eurjchem-267	198	41	n‐butanol	n‐butanol	PUNCT
eurjchem-267	198	42	and	and	CCONJ
eurjchem-267	198	43	by	by	ADP
eurjchem-267	198	44	heating	heat	VERB
eurjchem-267	198	45	2	2	NUM
eurjchem-267	198	46	above	above	ADP
eurjchem-267	198	47	its	its	PRON
eurjchem-267	198	48	melting	melting	NOUN
eurjchem-267	198	49	point	point	NOUN
eurjchem-267	198	50	to	to	PART
eurjchem-267	198	51	give	give	VERB
eurjchem-267	198	52	3	3	NUM
eurjchem-267	198	53	(	(	PUNCT
eurjchem-267	198	54	scheme	scheme	NOUN
eurjchem-267	198	55	1	1	NUM
eurjchem-267	198	56	)	)	PUNCT
eurjchem-267	198	57	.	.	PUNCT
eurjchem-267	199	1	when	when	SCONJ
eurjchem-267	199	2	1	1	NUM
eurjchem-267	199	3	was	be	AUX
eurjchem-267	199	4	allowed	allow	VERB
eurjchem-267	199	5	to	to	PART
eurjchem-267	199	6	react	react	VERB
eurjchem-267	199	7	with	with	ADP
eurjchem-267	199	8	7‐chlorobenzalazine	7‐chlorobenzalazine	NOUN
eurjchem-267	199	9	in	in	ADP
eurjchem-267	199	10	glacial	glacial	ADJ
eurjchem-267	199	11	acetic	acetic	ADJ
eurjchem-267	199	12	acid	acid	NOUN
eurjchem-267	199	13	containing	contain	VERB
eurjchem-267	199	14	catalytic	catalytic	ADJ
eurjchem-267	199	15	amount	amount	NOUN
eurjchem-267	199	16	of	of	ADP
eurjchem-267	199	17	anhydrous	anhydrous	ADJ
eurjchem-267	199	18	sodium	sodium	NOUN
eurjchem-267	199	19	acetate	acetate	NOUN
eurjchem-267	199	20	,	,	PUNCT
eurjchem-267	199	21	3‐(4‐chlorobenzylidene)amino‐2‐substituted	3‐(4‐chlorobenzylidene)amino‐2‐substituted	NUM
eurjchem-267	199	22	quinazolin‐4(h)‐one	quinazolin‐4(h)‐one	NOUN
eurjchem-267	199	23	(	(	PUNCT
eurjchem-267	199	24	4	4	NUM
eurjchem-267	199	25	)	)	PUNCT
eurjchem-267	199	26	was	be	AUX
eurjchem-267	199	27	isolated	isolate	VERB
eurjchem-267	199	28	as	as	ADP
eurjchem-267	199	29	the	the	DET
eurjchem-267	199	30	sole	sole	ADJ
eurjchem-267	199	31	product	product	NOUN
eurjchem-267	199	32	,	,	PUNCT
eurjchem-267	199	33	which	which	PRON
eurjchem-267	199	34	indicates	indicate	VERB
eurjchem-267	199	35	the	the	DET
eurjchem-267	199	36	displacement	displacement	NOUN
eurjchem-267	199	37	of	of	ADP
eurjchem-267	199	38	one	one	NUM
eurjchem-267	199	39	arylidene	arylidene	NOUN
eurjchem-267	199	40	group	group	NOUN
eurjchem-267	199	41	during	during	ADP
eurjchem-267	199	42	the	the	DET
eurjchem-267	199	43	reaction	reaction	NOUN
eurjchem-267	199	44	conditions	condition	NOUN
eurjchem-267	199	45	.	.	PUNCT
eurjchem-267	200	1	a	a	DET
eurjchem-267	200	2	possible	possible	ADJ
eurjchem-267	200	3	explanation	explanation	NOUN
eurjchem-267	200	4	for	for	ADP
eurjchem-267	200	5	the	the	DET
eurjchem-267	200	6	reaction	reaction	NOUN
eurjchem-267	200	7	of	of	ADP
eurjchem-267	200	8	1	1	NUM
eurjchem-267	200	9	with	with	ADP
eurjchem-267	200	10	the	the	DET
eurjchem-267	200	11	schiff	schiff	NOUN
eurjchem-267	200	12	’s	’s	PART
eurjchem-267	200	13	base	base	NOUN
eurjchem-267	200	14	and	and	CCONJ
eurjchem-267	200	15	azine	azine	NOUN
eurjchem-267	200	16	is	be	AUX
eurjchem-267	200	17	formulated	formulate	VERB
eurjchem-267	200	18	in	in	ADP
eurjchem-267	200	19	scheme	scheme	NOUN
eurjchem-267	200	20	2	2	NUM
eurjchem-267	200	21	.	.	PUNCT
eurjchem-267	201	1	the	the	DET
eurjchem-267	201	2	reaction	reaction	NOUN
eurjchem-267	201	3	of	of	ADP
eurjchem-267	201	4	1	1	NUM
eurjchem-267	201	5	with	with	ADP
eurjchem-267	201	6	the	the	DET
eurjchem-267	201	7	schiff	schiff	NOUN
eurjchem-267	201	8	’s	’s	PART
eurjchem-267	201	9	base	base	NOUN
eurjchem-267	201	10	and	and	CCONJ
eurjchem-267	201	11	azine	azine	NOUN
eurjchem-267	201	12	proceeded	proceed	VERB
eurjchem-267	201	13	via	via	ADP
eurjchem-267	201	14	the	the	DET
eurjchem-267	201	15	formation	formation	NOUN
eurjchem-267	201	16	of	of	ADP
eurjchem-267	201	17	the	the	DET
eurjchem-267	201	18	intermediate	intermediate	ADJ
eurjchem-267	201	19	(	(	PUNCT
eurjchem-267	201	20	z	z	NOUN
eurjchem-267	201	21	)	)	PUNCT
eurjchem-267	201	22	which	which	PRON
eurjchem-267	201	23	gave	give	VERB
eurjchem-267	201	24	rise	rise	NOUN
eurjchem-267	201	25	to	to	ADP
eurjchem-267	201	26	2	2	NUM
eurjchem-267	201	27	.	.	PUNCT
eurjchem-267	201	28	analogous	analogous	ADJ
eurjchem-267	201	29	intermediate	intermediate	ADJ
eurjchem-267	201	30	(	(	PUNCT
eurjchem-267	201	31	z	z	NOUN
eurjchem-267	201	32	)	)	PUNCT
eurjchem-267	201	33	have	have	AUX
eurjchem-267	201	34	been	be	AUX
eurjchem-267	201	35	reported	report	VERB
eurjchem-267	201	36	for	for	ADP
eurjchem-267	201	37	the	the	DET
eurjchem-267	201	38	reaction	reaction	NOUN
eurjchem-267	201	39	products	product	NOUN
eurjchem-267	201	40	of	of	ADP
eurjchem-267	201	41	imines	imine	NOUN
eurjchem-267	201	42	with	with	ADP
eurjchem-267	201	43	succinic	succinic	ADJ
eurjchem-267	201	44	and	and	CCONJ
eurjchem-267	201	45	maleic	maleic	ADJ
eurjchem-267	201	46	anhydrides	anhydride	NOUN
eurjchem-267	201	47	[	[	X
eurjchem-267	201	48	35	35	NUM
eurjchem-267	201	49	]	]	SYM
eurjchem-267	201	50	.	.	PUNCT
eurjchem-267	202	1	when	when	SCONJ
eurjchem-267	202	2	1	1	NUM
eurjchem-267	202	3	was	be	AUX
eurjchem-267	202	4	stirred	stir	VERB
eurjchem-267	202	5	with	with	ADP
eurjchem-267	202	6	hydrazine	hydrazine	NOUN
eurjchem-267	202	7	hydrate	hydrate	NOUN
eurjchem-267	202	8	(	(	PUNCT
eurjchem-267	202	9	80	80	NUM
eurjchem-267	202	10	%	%	NOUN
eurjchem-267	202	11	)	)	PUNCT
eurjchem-267	202	12	in	in	ADP
eurjchem-267	202	13	absolute	absolute	ADJ
eurjchem-267	202	14	ethanol	ethanol	NOUN
eurjchem-267	202	15	at	at	ADP
eurjchem-267	202	16	room	room	NOUN
eurjchem-267	202	17	temperature	temperature	NOUN
eurjchem-267	202	18	for	for	ADP
eurjchem-267	202	19	one	one	NUM
eurjchem-267	202	20	hour	hour	NOUN
eurjchem-267	202	21	,	,	PUNCT
eurjchem-267	202	22	the	the	DET
eurjchem-267	202	23	hydrazide	hydrazide	ADJ
eurjchem-267	202	24	derivative	derivative	ADJ
eurjchem-267	202	25	5	5	NUM
eurjchem-267	202	26	was	be	AUX
eurjchem-267	202	27	obtained	obtain	VERB
eurjchem-267	202	28	.	.	PUNCT
eurjchem-267	203	1	whereas	whereas	ADV
eurjchem-267	203	2	,	,	PUNCT
eurjchem-267	203	3	the	the	DET
eurjchem-267	203	4	same	same	ADJ
eurjchem-267	203	5	reaction	reaction	NOUN
eurjchem-267	203	6	under	under	ADP
eurjchem-267	203	7	relfux	relfux	NOUN
eurjchem-267	203	8	for	for	ADP
eurjchem-267	203	9	3	3	NUM
eurjchem-267	203	10	hrs	hrs	NOUN
eurjchem-267	203	11	afforded	afford	VERB
eurjchem-267	203	12	the	the	DET
eurjchem-267	203	13	3‐aminoquinazolin‐	3‐aminoquinazolin‐	NUM
eurjchem-267	203	14	4(h)‐one	4(h)‐one	NUM
eurjchem-267	203	15	derivative	derivative	ADJ
eurjchem-267	203	16	6	6	NUM
eurjchem-267	203	17	,	,	PUNCT
eurjchem-267	203	18	whose	whose	DET
eurjchem-267	203	19	structure	structure	NOUN
eurjchem-267	203	20	was	be	AUX
eurjchem-267	203	21	substantiated	substantiate	VERB
eurjchem-267	203	22	beside	beside	ADP
eurjchem-267	203	23	the	the	DET
eurjchem-267	203	24	correct	correct	ADJ
eurjchem-267	203	25	microanalytical	microanalytical	ADJ
eurjchem-267	203	26	and	and	CCONJ
eurjchem-267	203	27	spectroscopic	spectroscopic	ADJ
eurjchem-267	203	28	data	datum	NOUN
eurjchem-267	203	29	by	by	ADP
eurjchem-267	203	30	treatment	treatment	NOUN
eurjchem-267	203	31	compound	compound	NOUN
eurjchem-267	203	32	6	6	NUM
eurjchem-267	203	33	with	with	ADP
eurjchem-267	203	34	p‐chlorobenzaldehyde	p‐chlorobenzaldehyde	NOUN
eurjchem-267	203	35	in	in	ADP
eurjchem-267	203	36	refluxing	refluxing	NOUN
eurjchem-267	203	37	ethanol	ethanol	NOUN
eurjchem-267	203	38	to	to	PART
eurjchem-267	203	39	give	give	VERB
eurjchem-267	203	40	the	the	DET
eurjchem-267	203	41	quinazolinone	quinazolinone	NOUN
eurjchem-267	203	42	derivative	derivative	ADJ
eurjchem-267	203	43	4	4	NUM
eurjchem-267	203	44	(	(	PUNCT
eurjchem-267	203	45	scheme	scheme	NOUN
eurjchem-267	203	46	1	1	NUM
eurjchem-267	203	47	)	)	PUNCT
eurjchem-267	203	48	.	.	PUNCT
eurjchem-267	204	1	on	on	ADP
eurjchem-267	204	2	the	the	DET
eurjchem-267	204	3	other	other	ADJ
eurjchem-267	204	4	hand	hand	NOUN
eurjchem-267	204	5	,	,	PUNCT
eurjchem-267	204	6	treatment	treatment	NOUN
eurjchem-267	204	7	of	of	ADP
eurjchem-267	204	8	1	1	NUM
eurjchem-267	204	9	with	with	ADP
eurjchem-267	204	10	hydrazine	hydrazine	NOUN
eurjchem-267	204	11	hydrate	hydrate	NOUN
eurjchem-267	204	12	(	(	PUNCT
eurjchem-267	204	13	80	80	NUM
eurjchem-267	204	14	%	%	NOUN
eurjchem-267	204	15	)	)	PUNCT
eurjchem-267	204	16	in	in	ADP
eurjchem-267	204	17	boiling	boiling	NOUN
eurjchem-267	204	18	n‐butanol	n‐butanol	PUNCT
eurjchem-267	204	19	yielded	yield	VERB
eurjchem-267	204	20	the	the	DET
eurjchem-267	204	21	1,2,4‐triazino[6,1‐b]quinazolin‐	1,2,4‐triazino[6,1‐b]quinazolin‐	PROPN
eurjchem-267	204	22	10(4h)‐one	10(4h)‐one	NUM
eurjchem-267	204	23	derivative	derivative	ADJ
eurjchem-267	204	24	7	7	NUM
eurjchem-267	204	25	,	,	PUNCT
eurjchem-267	204	26	whose	whose	DET
eurjchem-267	204	27	structure	structure	NOUN
eurjchem-267	204	28	was	be	AUX
eurjchem-267	204	29	confirmed	confirm	VERB
eurjchem-267	204	30	from	from	ADP
eurjchem-267	204	31	the	the	DET
eurjchem-267	204	32	analytical	analytical	ADJ
eurjchem-267	204	33	and	and	CCONJ
eurjchem-267	204	34	spectral	spectral	ADJ
eurjchem-267	204	35	data	datum	NOUN
eurjchem-267	204	36	(	(	PUNCT
eurjchem-267	204	37	c.f	c.f	PROPN
eurjchem-267	204	38	.	.	PROPN
eurjchem-267	204	39	exp	exp	PROPN
eurjchem-267	204	40	.	.	PUNCT
eurjchem-267	204	41	)	)	PUNCT
eurjchem-267	204	42	.	.	PUNCT
eurjchem-267	205	1	similarly	similarly	ADV
eurjchem-267	205	2	,	,	PUNCT
eurjchem-267	205	3	the	the	DET
eurjchem-267	205	4	reaction	reaction	NOUN
eurjchem-267	205	5	of	of	ADP
eurjchem-267	205	6	1	1	NUM
eurjchem-267	205	7	with	with	ADP
eurjchem-267	205	8	hydroxyl	hydroxyl	NOUN
eurjchem-267	205	9	amine	amine	NOUN
eurjchem-267	205	10	in	in	ADP
eurjchem-267	205	11	order	order	NOUN
eurjchem-267	205	12	to	to	PART
eurjchem-267	205	13	obtain	obtain	VERB
eurjchem-267	205	14	another	another	DET
eurjchem-267	205	15	heterocyclic	heterocyclic	ADJ
eurjchem-267	205	16	ketone	ketone	NOUN
eurjchem-267	205	17	containing	contain	VERB
eurjchem-267	205	18	oxadiazine	oxadiazine	NOUN
eurjchem-267	205	19	nucleus	nucleus	PROPN
eurjchem-267	205	20	have	have	AUX
eurjchem-267	205	21	been	be	AUX
eurjchem-267	205	22	studied	study	VERB
eurjchem-267	205	23	.	.	PUNCT
eurjchem-267	206	1	thus	thus	ADV
eurjchem-267	206	2	,	,	PUNCT
eurjchem-267	206	3	treatment	treatment	NOUN
eurjchem-267	206	4	of	of	ADP
eurjchem-267	206	5	1	1	NUM
eurjchem-267	206	6	with	with	ADP
eurjchem-267	206	7	hydroxyl	hydroxyl	NOUN
eurjchem-267	206	8	amine	amine	ADJ
eurjchem-267	206	9	hydrochloride	hydrochloride	NOUN
eurjchem-267	206	10	in	in	ADP
eurjchem-267	206	11	refluxing	refluxing	NOUN
eurjchem-267	206	12	pyridine	pyridine	NOUN
eurjchem-267	206	13	afforded	afford	VERB
eurjchem-267	206	14	3‐hydroxy‐2‐	3‐hydroxy‐2‐	NUM
eurjchem-267	206	15	substituted	substitute	VERB
eurjchem-267	206	16	quinazolin‐4h‐one	quinazolin‐4h‐one	NOUN
eurjchem-267	206	17	8	8	NUM
eurjchem-267	206	18	,	,	PUNCT
eurjchem-267	206	19	which	which	PRON
eurjchem-267	206	20	spontaneously	spontaneously	ADV
eurjchem-267	206	21	recyclized	recyclize	VERB
eurjchem-267	206	22	in	in	ADP
eurjchem-267	206	23	freshly	freshly	ADV
eurjchem-267	206	24	distilled	distil	VERB
eurjchem-267	206	25	acetic	acetic	ADJ
eurjchem-267	206	26	anhydride	anhydride	NOUN
eurjchem-267	206	27	to	to	PART
eurjchem-267	206	28	give	give	VERB
eurjchem-267	206	29	the	the	DET
eurjchem-267	206	30	desired	desire	VERB
eurjchem-267	206	31	1,2,5‐oxadiazino[3,2‐b]quinazolin‐4(h)‐one	1,2,5‐oxadiazino[3,2‐b]quinazolin‐4(h)‐one	NUM
eurjchem-267	206	32	derivative	derivative	ADJ
eurjchem-267	206	33	9	9	NUM
eurjchem-267	206	34	(	(	PUNCT
eurjchem-267	206	35	scheme	scheme	NOUN
eurjchem-267	206	36	3	3	NUM
eurjchem-267	206	37	)	)	PUNCT
eurjchem-267	206	38	.	.	PUNCT
eurjchem-267	207	1	it	it	PRON
eurjchem-267	207	2	was	be	AUX
eurjchem-267	207	3	reported	report	VERB
eurjchem-267	207	4	[	[	X
eurjchem-267	207	5	37	37	NUM
eurjchem-267	207	6	]	]	PUNCT
eurjchem-267	207	7	that	that	SCONJ
eurjchem-267	207	8	the	the	DET
eurjchem-267	207	9	rate	rate	NOUN
eurjchem-267	207	10	of	of	ADP
eurjchem-267	207	11	addition	addition	NOUN
eurjchem-267	207	12	of	of	ADP
eurjchem-267	207	13	amines	amine	NOUN
eurjchem-267	207	14	to	to	ADP
eurjchem-267	207	15	the	the	DET
eurjchem-267	207	16	semiacid	semiacid	NOUN
eurjchem-267	207	17	anhydride	anhydride	NOUN
eurjchem-267	207	18	is	be	AUX
eurjchem-267	207	19	a	a	DET
eurjchem-267	207	20	function	function	NOUN
eurjchem-267	207	21	of	of	ADP
eurjchem-267	207	22	both	both	CCONJ
eurjchem-267	207	23	electronic	electronic	ADJ
eurjchem-267	207	24	as	as	ADV
eurjchem-267	207	25	well	well	ADV
eurjchem-267	207	26	as	as	ADP
eurjchem-267	207	27	steric	steric	ADJ
eurjchem-267	207	28	factors	factor	NOUN
eurjchem-267	207	29	and	and	CCONJ
eurjchem-267	207	30	the	the	DET
eurjchem-267	207	31	overall	overall	ADJ
eurjchem-267	207	32	rate	rate	NOUN
eurjchem-267	207	33	is	be	AUX
eurjchem-267	207	34	of	of	ADP
eurjchem-267	207	35	course	course	NOUN
eurjchem-267	207	36	affected	affect	VERB
eurjchem-267	207	37	by	by	ADP
eurjchem-267	207	38	ring	re	VERB
eurjchem-267	207	39	substituents	substituent	NOUN
eurjchem-267	207	40	that	that	PRON
eurjchem-267	207	41	influence	influence	VERB
eurjchem-267	207	42	the	the	DET
eurjchem-267	207	43	electrophilicity	electrophilicity	NOUN
eurjchem-267	207	44	at	at	ADP
eurjchem-267	207	45	position‐2	position‐2	ADV
eurjchem-267	207	46	,	,	PUNCT
eurjchem-267	207	47	so	so	SCONJ
eurjchem-267	207	48	addition	addition	NOUN
eurjchem-267	207	49	to	to	ADP
eurjchem-267	207	50	the	the	DET
eurjchem-267	207	51	more	more	ADV
eurjchem-267	207	52	electrophilic	electrophilic	ADJ
eurjchem-267	207	53	center	center	NOUN
eurjchem-267	207	54	at	at	ADP
eurjchem-267	207	55	position‐4	position‐4	ADV
eurjchem-267	207	56	may	may	AUX
eurjchem-267	207	57	occur	occur	VERB
eurjchem-267	207	58	faster	fast	ADV
eurjchem-267	207	59	.	.	PUNCT
eurjchem-267	208	1	the	the	DET
eurjchem-267	208	2	molarity	molarity	NOUN
eurjchem-267	208	3	of	of	ADP
eurjchem-267	208	4	amines	amine	NOUN
eurjchem-267	208	5	and	and	CCONJ
eurjchem-267	208	6	reaction	reaction	NOUN
eurjchem-267	208	7	time	time	NOUN
eurjchem-267	208	8	[	[	X
eurjchem-267	208	9	38	38	NUM
eurjchem-267	208	10	]	]	PUNCT
eurjchem-267	208	11	are	be	AUX
eurjchem-267	208	12	not	not	PART
eurjchem-267	208	13	the	the	DET
eurjchem-267	208	14	sole	sole	ADJ
eurjchem-267	208	15	factors	factor	NOUN
eurjchem-267	208	16	necessary	necessary	ADJ
eurjchem-267	208	17	for	for	ADP
eurjchem-267	208	18	cyclization	cyclization	NOUN
eurjchem-267	208	19	of	of	ADP
eurjchem-267	208	20	the	the	DET
eurjchem-267	208	21	anilide	anilide	ADJ
eurjchem-267	208	22	derivatives	derivative	NOUN
eurjchem-267	208	23	to	to	ADP
eurjchem-267	208	24	the	the	DET
eurjchem-267	208	25	corresponding	corresponding	ADJ
eurjchem-267	208	26	3‐substituted	3‐substitute	VERB
eurjchem-267	208	27	quinazoline	quinazoline	ADJ
eurjchem-267	208	28	derivatives	derivative	NOUN
eurjchem-267	208	29	.	.	PUNCT
eurjchem-267	209	1	however	however	ADV
eurjchem-267	209	2	,	,	PUNCT
eurjchem-267	209	3	the	the	DET
eurjchem-267	209	4	reaction	reaction	NOUN
eurjchem-267	209	5	of	of	ADP
eurjchem-267	209	6	1	1	NUM
eurjchem-267	209	7	with	with	ADP
eurjchem-267	209	8	benzidine	benzidine	NOUN
eurjchem-267	209	9	in	in	ADP
eurjchem-267	209	10	n‐	n‐	NOUN
eurjchem-267	209	11	butanol	butanol	NOUN
eurjchem-267	209	12	furnished	furnish	VERB
eurjchem-267	209	13	the	the	DET
eurjchem-267	209	14	cyclized	cyclized	ADJ
eurjchem-267	209	15	product	product	NOUN
eurjchem-267	209	16	10	10	NUM
eurjchem-267	209	17	.	.	PUNCT
eurjchem-267	209	18	fusion	fusion	NOUN
eurjchem-267	209	19	of	of	ADP
eurjchem-267	209	20	1	1	NUM
eurjchem-267	209	21	with	with	ADP
eurjchem-267	209	22	o‐	o‐	PROPN
eurjchem-267	209	23	phenylenediamine	phenylenediamine	NOUN
eurjchem-267	209	24	in	in	ADP
eurjchem-267	209	25	an	an	DET
eurjchem-267	209	26	oil‐bath	oil‐bath	NOUN
eurjchem-267	209	27	at	at	ADP
eurjchem-267	209	28	190	190	NUM
eurjchem-267	209	29	oc	oc	AUX
eurjchem-267	209	30	afforded	afford	VERB
eurjchem-267	209	31	the	the	DET
eurjchem-267	209	32	benzimidazolo[1,2‐c]quinazoline	benzimidazolo[1,2‐c]quinazoline	PROPN
eurjchem-267	209	33	derivative	derivative	ADJ
eurjchem-267	209	34	11	11	NUM
eurjchem-267	209	35	.	.	PUNCT
eurjchem-267	210	1	furthermore	furthermore	ADV
eurjchem-267	210	2	,	,	PUNCT
eurjchem-267	210	3	refluxing	refluxing	NOUN
eurjchem-267	210	4	1	1	NUM
eurjchem-267	210	5	with	with	ADP
eurjchem-267	210	6	n‐(1‐naphthyl)ethylene‐diamine	n‐(1‐naphthyl)ethylene‐diamine	NOUN
eurjchem-267	210	7	hydro‐	hydro‐	X
eurjchem-267	210	8	chloride	chloride	NOUN
eurjchem-267	210	9	in	in	ADP
eurjchem-267	210	10	pyridine	pyridine	NOUN
eurjchem-267	210	11	yielded	yield	VERB
eurjchem-267	210	12	the	the	DET
eurjchem-267	210	13	quinazolin‐4(h)‐one	quinazolin‐4(h)‐one	PROPN
eurjchem-267	210	14	derivative	derivative	ADJ
eurjchem-267	210	15	12	12	NUM
eurjchem-267	210	16	.	.	PUNCT
eurjchem-267	211	1	upon	upon	SCONJ
eurjchem-267	211	2	treatment	treatment	NOUN
eurjchem-267	211	3	of	of	ADP
eurjchem-267	211	4	1	1	NUM
eurjchem-267	211	5	with	with	ADP
eurjchem-267	211	6	2‐aminopyridine	2‐aminopyridine	NUM
eurjchem-267	211	7	in	in	ADP
eurjchem-267	211	8	boiling	boiling	NOUN
eurjchem-267	211	9	ethanol	ethanol	NOUN
eurjchem-267	211	10	or	or	CCONJ
eurjchem-267	211	11	n‐butanol	n‐butanol	ADV
eurjchem-267	211	12	,	,	PUNCT
eurjchem-267	211	13	1	1	NUM
eurjchem-267	211	14	was	be	AUX
eurjchem-267	211	15	recovered	recover	VERB
eurjchem-267	211	16	unchanged	unchanged	ADJ
eurjchem-267	211	17	.	.	PUNCT
eurjchem-267	212	1	however	however	ADV
eurjchem-267	212	2	,	,	PUNCT
eurjchem-267	212	3	heating	heat	VERB
eurjchem-267	212	4	1	1	NUM
eurjchem-267	212	5	with	with	ADP
eurjchem-267	212	6	2‐aminopyridine	2‐aminopyridine	NUM
eurjchem-267	212	7	in	in	ADP
eurjchem-267	212	8	an	an	DET
eurjchem-267	212	9	oil‐bath	oil‐bath	NOUN
eurjchem-267	212	10	at	at	ADP
eurjchem-267	212	11	200	200	NUM
eurjchem-267	212	12	oc	oc	NOUN
eurjchem-267	212	13	gave	give	VERB
eurjchem-267	212	14	the	the	DET
eurjchem-267	212	15	quinazolin‐4(h)‐one	quinazolin‐4(h)‐one	PROPN
eurjchem-267	212	16	derivative	derivative	ADJ
eurjchem-267	212	17	13	13	NUM
eurjchem-267	212	18	(	(	PUNCT
eurjchem-267	212	19	scheme	scheme	NOUN
eurjchem-267	212	20	3	3	NUM
eurjchem-267	212	21	)	)	PUNCT
eurjchem-267	212	22	.	.	PUNCT
eurjchem-267	213	1	references	reference	NOUN
eurjchem-267	213	2	[	[	X
eurjchem-267	213	3	1	1	NUM
eurjchem-267	213	4	]	]	PUNCT
eurjchem-267	213	5	.	.	PUNCT
eurjchem-267	214	1	tang	tang	PROPN
eurjchem-267	214	2	,	,	PUNCT
eurjchem-267	214	3	c.	c.	PROPN
eurjchem-267	214	4	;	;	PUNCT
eurjchem-267	214	5	chang	chang	PROPN
eurjchem-267	214	6	,	,	PUNCT
eurjchem-267	214	7	s.	s.	PROPN
eurjchem-267	214	8	h.	h.	PROPN
eurjchem-267	214	9	;	;	PUNCT
eurjchem-267	214	10	hoo	hoo	PROPN
eurjchem-267	214	11	,	,	PUNCT
eurjchem-267	214	12	d.	d.	PROPN
eurjchem-267	214	13	;	;	PUNCT
eurjchem-267	214	14	yanagihara	yanagihara	PROPN
eurjchem-267	214	15	,	,	PUNCT
eurjchem-267	214	16	k.	k.	PROPN
eurjchem-267	214	17	h.	h.	PROPN
eurjchem-267	214	18	phytochemistry	phytochemistry	PROPN
eurjchem-267	214	19	1975	1975	NUM
eurjchem-267	214	20	,	,	PUNCT
eurjchem-267	214	21	14	14	NUM
eurjchem-267	214	22	,	,	PUNCT
eurjchem-267	214	23	2077‐2079	2077‐2079	NUM
eurjchem-267	214	24	.	.	PUNCT
eurjchem-267	215	1	[	[	X
eurjchem-267	215	2	2	2	NUM
eurjchem-267	215	3	]	]	PUNCT
eurjchem-267	215	4	.	.	PUNCT
eurjchem-267	216	1	argandona	argandona	PROPN
eurjchem-267	216	2	,	,	PUNCT
eurjchem-267	216	3	v.	v.	PROPN
eurjchem-267	216	4	h.	h.	PROPN
eurjchem-267	216	5	;	;	PUNCT
eurjchem-267	216	6	corcuera	corcuera	NOUN
eurjchem-267	216	7	,	,	PUNCT
eurjchem-267	216	8	l.	l.	PROPN
eurjchem-267	216	9	j.	j.	PROPN
eurjchem-267	216	10	;	;	PUNCT
eurjchem-267	216	11	niemeyer	niemeyer	PROPN
eurjchem-267	216	12	,	,	PUNCT
eurjchem-267	216	13	h.	h.	PROPN
eurjchem-267	216	14	m.	m.	PROPN
eurjchem-267	216	15	;	;	PUNCT
eurjchem-267	216	16	campbell	campbell	PROPN
eurjchem-267	216	17	,	,	PUNCT
eurjchem-267	216	18	b.	b.	PROPN
eurjchem-267	216	19	c.	c.	PROPN
eurjchem-267	216	20	entomol	entomol	PROPN
eurjchem-267	216	21	.	.	PUNCT
eurjchem-267	217	1	exp	exp	PROPN
eurjchem-267	217	2	.	.	PUNCT
eurjchem-267	217	3	appl	appl	PROPN
eurjchem-267	217	4	.	.	PROPN
eurjchem-267	218	1	1983	1983	NUM
eurjchem-267	218	2	,	,	PUNCT
eurjchem-267	218	3	34	34	NUM
eurjchem-267	218	4	,	,	PUNCT
eurjchem-267	218	5	134‐138	134‐138	NUM
eurjchem-267	218	6	.	.	PUNCT
eurjchem-267	219	1	[	[	X
eurjchem-267	219	2	3	3	NUM
eurjchem-267	219	3	]	]	PUNCT
eurjchem-267	219	4	.	.	PUNCT
eurjchem-267	220	1	bravo	bravo	PROPN
eurjchem-267	220	2	,	,	PUNCT
eurjchem-267	220	3	h.	h.	PROPN
eurjchem-267	220	4	r.	r.	PROPN
eurjchem-267	220	5	;	;	PUNCT
eurjchem-267	220	6	lazo	lazo	PROPN
eurjchem-267	220	7	,	,	PUNCT
eurjchem-267	220	8	w.	w.	PROPN
eurjchem-267	220	9	j.	j.	PROPN
eurjchem-267	220	10	agric	agric	PROPN
eurjchem-267	220	11	.	.	PUNCT
eurjchem-267	221	1	food	food	NOUN
eurjchem-267	221	2	chem	chem	NOUN
eurjchem-267	221	3	.	.	PUNCT
eurjchem-267	222	1	1996	1996	NUM
eurjchem-267	222	2	,	,	PUNCT
eurjchem-267	222	3	44	44	NUM
eurjchem-267	222	4	,	,	PUNCT
eurjchem-267	222	5	1569‐1571	1569‐1571	NUM
eurjchem-267	222	6	.	.	PUNCT
eurjchem-267	223	1	[	[	X
eurjchem-267	223	2	4	4	NUM
eurjchem-267	223	3	]	]	PUNCT
eurjchem-267	223	4	.	.	PUNCT
eurjchem-267	223	5	sicker	sicker	PROPN
eurjchem-267	223	6	,	,	PUNCT
eurjchem-267	223	7	d.	d.	PROPN
eurjchem-267	223	8	;	;	PUNCT
eurjchem-267	223	9	frey	frey	PROPN
eurjchem-267	223	10	,	,	PUNCT
eurjchem-267	223	11	m.	m.	NOUN
eurjchem-267	223	12	;	;	PUNCT
eurjchem-267	223	13	schulz	schulz	PROPN
eurjchem-267	223	14	,	,	PUNCT
eurjchem-267	223	15	m.	m.	NOUN
eurjchem-267	223	16	;	;	PUNCT
eurjchem-267	223	17	gierl	gierl	NOUN
eurjchem-267	223	18	,	,	PUNCT
eurjchem-267	223	19	a.	a.	PROPN
eurjchem-267	223	20	inc	inc	PROPN
eurjchem-267	223	21	.	.	PROPN
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eurjchem-267	224	2	.	.	PUNCT
eurjchem-267	225	1	2000	2000	NUM
eurjchem-267	225	2	,	,	PUNCT
eurjchem-267	225	3	198	198	NUM
eurjchem-267	225	4	,	,	PUNCT
eurjchem-267	225	5	319‐	319‐	NUM
eurjchem-267	225	6	346	346	NUM
eurjchem-267	225	7	.	.	PUNCT
eurjchem-267	226	1	[	[	X
eurjchem-267	226	2	5	5	NUM
eurjchem-267	226	3	]	]	PUNCT
eurjchem-267	226	4	.	.	PUNCT
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eurjchem-267	227	2	,	,	PUNCT
eurjchem-267	227	3	f.	f.	PROPN
eurjchem-267	227	4	a.	a.	PROPN
eurjchem-267	227	5	;	;	PUNCT
eurjchem-267	227	6	marin	marin	PROPN
eurjchem-267	227	7	,	,	PUNCT
eurjchem-267	227	8	d.	d.	PROPN
eurjchem-267	227	9	;	;	PUNCT
eurjchem-267	227	10	oliveros‐bastidas	oliveros‐bastidas	PROPN
eurjchem-267	227	11	,	,	PUNCT
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eurjchem-267	227	13	;	;	PUNCT
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eurjchem-267	227	19	,	,	PUNCT
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eurjchem-267	227	22	;	;	PUNCT
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eurjchem-267	227	26	m.	m.	PROPN
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eurjchem-267	227	28	j.	j.	PROPN
eurjchem-267	227	29	agric	agric	PROPN
eurjchem-267	227	30	.	.	PUNCT
eurjchem-267	228	1	food	food	NOUN
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eurjchem-267	228	3	.	.	PUNCT
eurjchem-267	229	1	2005	2005	NUM
eurjchem-267	229	2	,	,	PUNCT
eurjchem-267	229	3	53	53	NUM
eurjchem-267	229	4	,	,	PUNCT
eurjchem-267	229	5	538‐548	538‐548	NUM
eurjchem-267	229	6	.	.	PUNCT
eurjchem-267	230	1	[	[	X
eurjchem-267	230	2	6	6	NUM
eurjchem-267	230	3	]	]	PUNCT
eurjchem-267	230	4	.	.	PUNCT
eurjchem-267	231	1	macias	macias	PROPN
eurjchem-267	231	2	,	,	PUNCT
eurjchem-267	231	3	f.	f.	PROPN
eurjchem-267	231	4	a.	a.	PROPN
eurjchem-267	231	5	;	;	PUNCT
eurjchem-267	231	6	marin	marin	PROPN
eurjchem-267	231	7	,	,	PUNCT
eurjchem-267	231	8	d.	d.	PROPN
eurjchem-267	231	9	;	;	PUNCT
eurjchem-267	231	10	oliveros‐bastidas	oliveros‐bastidas	PROPN
eurjchem-267	231	11	,	,	PUNCT
eurjchem-267	231	12	a.	a.	NOUN
eurjchem-267	231	13	;	;	PUNCT
eurjchem-267	231	14	chinchilla	chinchilla	X
eurjchem-267	231	15	,	,	PUNCT
eurjchem-267	231	16	d.	d.	PROPN
eurjchem-267	231	17	;	;	PUNCT
eurjchem-267	231	18	simonet	simonet	PROPN
eurjchem-267	231	19	,	,	PUNCT
eurjchem-267	231	20	a.	a.	NOUN
eurjchem-267	231	21	m.	m.	NOUN
eurjchem-267	231	22	;	;	PUNCT
eurjchem-267	231	23	molinillo	molinillo	PROPN
eurjchem-267	231	24	,	,	PUNCT
eurjchem-267	231	25	j.	j.	PROPN
eurjchem-267	231	26	m.	m.	PROPN
eurjchem-267	231	27	c.	c.	PROPN
eurjchem-267	231	28	j.	j.	PROPN
eurjchem-267	231	29	agric	agric	PROPN
eurjchem-267	231	30	.	.	PUNCT
eurjchem-267	232	1	food	food	NOUN
eurjchem-267	232	2	chem	chem	NOUN
eurjchem-267	232	3	.	.	PUNCT
eurjchem-267	233	1	2006	2006	NUM
eurjchem-267	233	2	,	,	PUNCT
eurjchem-267	233	3	54	54	NUM
eurjchem-267	233	4	,	,	PUNCT
eurjchem-267	233	5	991‐1000	991‐1000	NUM
eurjchem-267	233	6	.	.	PUNCT
eurjchem-267	234	1	[	[	X
eurjchem-267	234	2	7	7	NUM
eurjchem-267	234	3	]	]	PUNCT
eurjchem-267	234	4	.	.	PUNCT
eurjchem-267	235	1	macias	macias	PROPN
eurjchem-267	235	2	,	,	PUNCT
eurjchem-267	235	3	f.	f.	PROPN
eurjchem-267	235	4	a.	a.	PROPN
eurjchem-267	235	5	;	;	PUNCT
eurjchem-267	235	6	marin	marin	PROPN
eurjchem-267	235	7	,	,	PUNCT
eurjchem-267	235	8	d.	d.	PROPN
eurjchem-267	235	9	;	;	PUNCT
eurjchem-267	235	10	oliveros‐bastidas	oliveros‐bastidas	PROPN
eurjchem-267	235	11	,	,	PUNCT
eurjchem-267	235	12	a.	a.	NOUN
eurjchem-267	235	13	;	;	PUNCT
eurjchem-267	235	14	molinillo	molinillo	PROPN
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eurjchem-267	235	16	j.	j.	PROPN
eurjchem-267	235	17	m.	m.	PROPN
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eurjchem-267	235	19	j.	j.	PROPN
eurjchem-267	235	20	agric	agric	PROPN
eurjchem-267	235	21	.	.	PUNCT
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eurjchem-267	236	3	.	.	PUNCT
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eurjchem-267	237	2	,	,	PUNCT
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eurjchem-267	237	4	,	,	PUNCT
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eurjchem-267	237	6	.	.	PUNCT
eurjchem-267	238	1	[	[	X
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eurjchem-267	238	3	]	]	PUNCT
eurjchem-267	238	4	.	.	PUNCT
eurjchem-267	239	1	macias	macias	PROPN
eurjchem-267	239	2	,	,	PUNCT
eurjchem-267	239	3	f.	f.	PROPN
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eurjchem-267	239	5	;	;	PUNCT
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eurjchem-267	239	8	,	,	PUNCT
eurjchem-267	239	9	j.	j.	PROPN
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eurjchem-267	239	17	,	,	PUNCT
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eurjchem-267	239	21	,	,	PUNCT
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eurjchem-267	240	3	.	.	PUNCT
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eurjchem-267	241	2	,	,	PUNCT
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eurjchem-267	241	4	,	,	PUNCT
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eurjchem-267	241	6	.	.	PUNCT
eurjchem-267	242	1	[	[	X
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eurjchem-267	242	3	]	]	PUNCT
eurjchem-267	242	4	.	.	PUNCT
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eurjchem-267	243	9	.	.	PUNCT
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eurjchem-267	243	11	.	.	PUNCT
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eurjchem-267	244	2	,	,	PUNCT
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eurjchem-267	244	4	,	,	PUNCT
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eurjchem-267	244	6	.	.	PUNCT
eurjchem-267	245	1	[	[	X
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eurjchem-267	245	3	]	]	PUNCT
eurjchem-267	245	4	.	.	PUNCT
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eurjchem-267	246	2	,	,	PUNCT
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eurjchem-267	246	4	;	;	PUNCT
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eurjchem-267	246	6	,	,	PUNCT
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eurjchem-267	246	8	;	;	PUNCT
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eurjchem-267	246	10	,	,	PUNCT
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eurjchem-267	246	12	;	;	PUNCT
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eurjchem-267	246	14	,	,	PUNCT
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eurjchem-267	246	18	,	,	PUNCT
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eurjchem-267	246	20	,	,	PUNCT
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eurjchem-267	246	22	.	.	PUNCT
eurjchem-267	247	1	[	[	X
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eurjchem-267	247	3	]	]	PUNCT
eurjchem-267	247	4	.	.	PUNCT
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eurjchem-267	247	6	,	,	PUNCT
eurjchem-267	247	7	n.	n.	PROPN
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eurjchem-267	247	9	;	;	PUNCT
eurjchem-267	247	10	thampi	thampi	ADJ
eurjchem-267	247	11	,	,	PUNCT
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eurjchem-267	247	13	;	;	PUNCT
eurjchem-267	247	14	gurubasavarajaswamy	gurubasavarajaswamy	NOUN
eurjchem-267	247	15	,	,	PUNCT
eurjchem-267	247	16	p.	p.	NOUN
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eurjchem-267	247	20	,	,	PUNCT
eurjchem-267	247	21	d.	d.	PROPN
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eurjchem-267	247	26	,	,	PUNCT
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eurjchem-267	247	28	,	,	PUNCT
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eurjchem-267	247	30	.	.	PUNCT
eurjchem-267	248	1	[	[	X
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eurjchem-267	248	3	]	]	PUNCT
eurjchem-267	248	4	.	.	PUNCT
eurjchem-267	249	1	gao	gao	PROPN
eurjchem-267	249	2	,	,	PUNCT
eurjchem-267	249	3	x.	x.	PROPN
eurjchem-267	249	4	;	;	PUNCT
eurjchem-267	249	5	cai	cai	X
eurjchem-267	249	6	,	,	PUNCT
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eurjchem-267	249	8	;	;	PUNCT
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eurjchem-267	249	10	,	,	PUNCT
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eurjchem-267	249	12	;	;	PUNCT
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eurjchem-267	249	14	,	,	PUNCT
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eurjchem-267	249	18	,	,	PUNCT
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eurjchem-267	249	20	;	;	PUNCT
eurjchem-267	249	21	chen	chen	PROPN
eurjchem-267	249	22	,	,	PUNCT
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eurjchem-267	249	26	,	,	PUNCT
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eurjchem-267	249	28	,	,	PUNCT
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eurjchem-267	249	30	.	.	PUNCT
eurjchem-267	250	1	[	[	X
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eurjchem-267	250	3	]	]	PUNCT
eurjchem-267	250	4	.	.	PUNCT
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eurjchem-267	251	2	,	,	PUNCT
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eurjchem-267	251	6	;	;	PUNCT
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eurjchem-267	251	8	,	,	PUNCT
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eurjchem-267	251	10	;	;	PUNCT
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eurjchem-267	251	12	,	,	PUNCT
eurjchem-267	251	13	e.	e.	PROPN
eurjchem-267	251	14	;	;	PUNCT
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eurjchem-267	251	16	,	,	PUNCT
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eurjchem-267	251	18	;	;	PUNCT
eurjchem-267	251	19	besson	besson	PROPN
eurjchem-267	251	20	,	,	PUNCT
eurjchem-267	251	21	t.	t.	PROPN
eurjchem-267	251	22	j.	j.	PROPN
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eurjchem-267	251	24	.	.	PUNCT
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eurjchem-267	252	2	.	.	PUNCT
eurjchem-267	253	1	med	med	PROPN
eurjchem-267	253	2	.	.	PROPN
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eurjchem-267	253	4	.	.	PUNCT
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eurjchem-267	254	2	,	,	PUNCT
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eurjchem-267	254	4	,	,	PUNCT
eurjchem-267	254	5	577‐583	577‐583	NUM
eurjchem-267	254	6	.	.	PUNCT
eurjchem-267	255	1	[	[	X
eurjchem-267	255	2	14	14	NUM
eurjchem-267	255	3	]	]	PUNCT
eurjchem-267	255	4	.	.	PUNCT
eurjchem-267	256	1	abu‐shady	abu‐shady	PROPN
eurjchem-267	256	2	,	,	PUNCT
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eurjchem-267	256	5	;	;	PUNCT
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eurjchem-267	256	7	,	,	PUNCT
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eurjchem-267	256	10	;	;	PUNCT
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eurjchem-267	256	12	,	,	PUNCT
eurjchem-267	256	13	s.	s.	PROPN
eurjchem-267	256	14	e.	e.	PROPN
eurjchem-267	256	15	;	;	PUNCT
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eurjchem-267	256	17	,	,	PUNCT
eurjchem-267	256	18	h.	h.	PROPN
eurjchem-267	256	19	e.	e.	PROPN
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eurjchem-267	256	21	.	.	PUNCT
eurjchem-267	257	1	j.	j.	PROPN
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eurjchem-267	257	3	.	.	PUNCT
eurjchem-267	258	1	2007	2007	NUM
eurjchem-267	258	2	,	,	PUNCT
eurjchem-267	258	3	50(3	50(3	NUM
eurjchem-267	258	4	)	)	PUNCT
eurjchem-267	258	5	,	,	PUNCT
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eurjchem-267	258	7	.	.	PUNCT
eurjchem-267	259	1	[	[	X
eurjchem-267	259	2	15	15	NUM
eurjchem-267	259	3	]	]	PUNCT
eurjchem-267	259	4	.	.	PUNCT
eurjchem-267	260	1	kumar	kumar	PROPN
eurjchem-267	260	2	,	,	PUNCT
eurjchem-267	260	3	a.	a.	PROPN
eurjchem-267	260	4	;	;	PUNCT
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eurjchem-267	260	6	,	,	PUNCT
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eurjchem-267	260	15	.	.	PUNCT
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eurjchem-267	261	4	.	.	PUNCT
eurjchem-267	262	1	2007	2007	NUM
eurjchem-267	262	2	,	,	PUNCT
eurjchem-267	262	3	15	15	NUM
eurjchem-267	262	4	,	,	PUNCT
eurjchem-267	262	5	3089‐	3089‐	NUM
eurjchem-267	262	6	3096	3096	NUM
eurjchem-267	262	7	.	.	PUNCT
eurjchem-267	263	1	[	[	X
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eurjchem-267	263	4	.	.	PUNCT
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eurjchem-267	264	2	,	,	PUNCT
eurjchem-267	264	3	p.	p.	PROPN
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eurjchem-267	264	5	tarraga	tarraga	PROPN
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eurjchem-267	264	8	;	;	PUNCT
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eurjchem-267	264	16	;	;	PUNCT
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eurjchem-267	264	18	,	,	PUNCT
eurjchem-267	264	19	a.	a.	NOUN
eurjchem-267	264	20	;	;	PUNCT
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eurjchem-267	264	22	,	,	PUNCT
eurjchem-267	264	23	m.	m.	NOUN
eurjchem-267	264	24	c.	c.	PROPN
eurjchem-267	264	25	;	;	PUNCT
eurjchem-267	264	26	alcaraz	alcaraz	NOUN
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eurjchem-267	264	29	j.	j.	PROPN
eurjchem-267	264	30	j.	j.	PROPN
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eurjchem-267	265	1	prod	prod	PROPN
eurjchem-267	265	2	.	.	PUNCT
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eurjchem-267	266	2	,	,	PUNCT
eurjchem-267	266	3	64	64	NUM
eurjchem-267	266	4	,	,	PUNCT
eurjchem-267	266	5	1297‐1300	1297‐1300	NUM
eurjchem-267	266	6	.	.	PUNCT
eurjchem-267	267	1	[	[	X
eurjchem-267	267	2	17	17	NUM
eurjchem-267	267	3	]	]	PUNCT
eurjchem-267	267	4	.	.	PUNCT
eurjchem-267	268	1	de	de	X
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eurjchem-267	268	3	,	,	PUNCT
eurjchem-267	268	4	s.	s.	PROPN
eurjchem-267	268	5	e.	e.	PROPN
eurjchem-267	268	6	;	;	PUNCT
eurjchem-267	268	7	quagliato	quagliato	PROPN
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eurjchem-267	268	13	,	,	PUNCT
eurjchem-267	268	14	w.	w.	PROPN
eurjchem-267	268	15	j.	j.	PROPN
eurjchem-267	268	16	;	;	PUNCT
eurjchem-267	268	17	patchett	patchett	PROPN
eurjchem-267	268	18	,	,	PUNCT
eurjchem-267	268	19	a.	a.	NOUN
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eurjchem-267	268	21	;	;	PUNCT
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eurjchem-267	268	25	s.	s.	PROPN
eurjchem-267	268	26	l.	l.	PROPN
eurjchem-267	268	27	;	;	PUNCT
eurjchem-267	268	28	lotti	lotti	PROPN
eurjchem-267	268	29	,	,	PUNCT
eurjchem-267	268	30	v.	v.	PROPN
eurjchem-267	268	31	j.	j.	PROPN
eurjchem-267	268	32	;	;	PUNCT
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eurjchem-267	268	38	scheck	scheck	PROPN
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eurjchem-267	268	40	s.	s.	PROPN
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eurjchem-267	268	44	,	,	PUNCT
eurjchem-267	268	45	k.	k.	PROPN
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eurjchem-267	268	50	s.	s.	PROPN
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eurjchem-267	268	53	schorn	schorn	VERB
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eurjchem-267	268	55	t.	t.	PROPN
eurjchem-267	268	56	s.	s.	PROPN
eurjchem-267	268	57	;	;	PUNCT
eurjchem-267	268	58	zingaro	zingaro	NOUN
eurjchem-267	268	59	,	,	PUNCT
eurjchem-267	268	60	g.	g.	PROPN
eurjchem-267	268	61	j.	j.	PROPN
eurjchem-267	268	62	;	;	PUNCT
eurjchem-267	268	63	siegl	siegl	PROPN
eurjchem-267	268	64	,	,	PUNCT
eurjchem-267	269	1	p.	p.	PROPN
eurjchem-267	269	2	k.	k.	PROPN
eurjchem-267	270	1	s.	s.	PROPN
eurjchem-267	270	2	j.	j.	PROPN
eurjchem-267	270	3	med	med	PROPN
eurjchem-267	270	4	.	.	PROPN
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eurjchem-267	270	6	.	.	PUNCT
eurjchem-267	271	1	1993	1993	NUM
eurjchem-267	271	2	,	,	PUNCT
eurjchem-267	271	3	36	36	NUM
eurjchem-267	271	4	,	,	PUNCT
eurjchem-267	271	5	3207‐	3207‐	NUM
eurjchem-267	271	6	3210	3210	NUM
eurjchem-267	271	7	.	.	PUNCT
eurjchem-267	272	1	[	[	X
eurjchem-267	272	2	18	18	NUM
eurjchem-267	272	3	]	]	PUNCT
eurjchem-267	272	4	.	.	PUNCT
eurjchem-267	273	1	koizumi	koizumi	PROPN
eurjchem-267	273	2	,	,	PUNCT
eurjchem-267	273	3	m.	m.	NOUN
eurjchem-267	273	4	;	;	PUNCT
eurjchem-267	273	5	matsuura	matsuura	PROPN
eurjchem-267	273	6	,	,	PUNCT
eurjchem-267	273	7	i.	i.	PROPN
eurjchem-267	273	8	;	;	PUNCT
eurjchem-267	273	9	murakami	murakami	NOUN
eurjchem-267	273	10	,	,	PUNCT
eurjchem-267	273	11	y.	y.	PROPN
eurjchem-267	273	12	;	;	PUNCT
eurjchem-267	273	13	japan	japan	PROPN
eurjchem-267	273	14	kokai	kokai	PROPN
eurjchem-267	273	15	77	77	NUM
eurjchem-267	273	16	77	77	NUM
eurjchem-267	273	17	,	,	PUNCT
eurjchem-267	273	18	093	093	NUM
eurjchem-267	273	19	,	,	PUNCT
eurjchem-267	273	20	1977	1977	NUM
eurjchem-267	273	21	(	(	PUNCT
eurjchem-267	273	22	c.	c.	PROPN
eurjchem-267	273	23	a.	a.	PROPN
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eurjchem-267	273	25	,	,	PUNCT
eurjchem-267	273	26	88	88	NUM
eurjchem-267	273	27	,	,	PUNCT
eurjchem-267	273	28	6930s	6930s	NUM
eurjchem-267	273	29	)	)	PUNCT
eurjchem-267	273	30	.	.	PUNCT
eurjchem-267	274	1	[	[	X
eurjchem-267	274	2	19	19	NUM
eurjchem-267	274	3	]	]	PUNCT
eurjchem-267	274	4	.	.	PUNCT
eurjchem-267	275	1	liu	liu	PROPN
eurjchem-267	275	2	,	,	PUNCT
eurjchem-267	275	3	j‐f	j‐f	PRON
eurjchem-267	275	4	;	;	PUNCT
eurjchem-267	275	5	ye	ye	PRON
eurjchem-267	275	6	,	,	PUNCT
eurjchem-267	275	7	p.	p.	NOUN
eurjchem-267	275	8	;	;	PUNCT
eurjchem-267	275	9	sprague	sprague	PROPN
eurjchem-267	275	10	,	,	PUNCT
eurjchem-267	275	11	k.	k.	PROPN
eurjchem-267	275	12	;	;	PUNCT
eurjchem-267	275	13	sargent	sargent	PROPN
eurjchem-267	275	14	,	,	PUNCT
eurjchem-267	275	15	k.	k.	PROPN
eurjchem-267	275	16	;	;	PUNCT
eurjchem-267	275	17	yohannes	yohanne	NOUN
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eurjchem-267	275	19	d.	d.	PROPN
eurjchem-267	275	20	;	;	PUNCT
eurjchem-267	275	21	baldino	baldino	PROPN
eurjchem-267	275	22	,	,	PUNCT
eurjchem-267	275	23	c.	c.	PROPN
eurjchem-267	275	24	m.	m.	NOUN
eurjchem-267	275	25	;	;	PUNCT
eurjchem-267	275	26	wilson	wilson	PROPN
eurjchem-267	275	27	,	,	PUNCT
eurjchem-267	275	28	c.	c.	PROPN
eurjchem-267	275	29	j.	j.	PROPN
eurjchem-267	275	30	;	;	PUNCT
eurjchem-267	275	31	ng	ng	PROPN
eurjchem-267	275	32	,	,	PUNCT
eurjchem-267	275	33	s‐c	s‐c	PROPN
eurjchem-267	275	34	.	.	PUNCT
eurjchem-267	276	1	org	org	PROPN
eurjchem-267	276	2	.	.	PUNCT
eurjchem-267	277	1	lett	lett	PROPN
eurjchem-267	277	2	.	.	PUNCT
eurjchem-267	278	1	2005	2005	NUM
eurjchem-267	278	2	,	,	PUNCT
eurjchem-267	278	3	7	7	NUM
eurjchem-267	278	4	,	,	PUNCT
eurjchem-267	278	5	3363‐3366	3363‐3366	NUM
eurjchem-267	278	6	.	.	PUNCT
eurjchem-267	279	1	[	[	X
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eurjchem-267	279	3	]	]	PUNCT
eurjchem-267	279	4	.	.	PUNCT
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eurjchem-267	280	2	,	,	PUNCT
eurjchem-267	280	3	a.	a.	PROPN
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eurjchem-267	280	5	a.	a.	PROPN
eurjchem-267	280	6	;	;	PUNCT
eurjchem-267	280	7	hafez	hafez	PROPN
eurjchem-267	280	8	,	,	PUNCT
eurjchem-267	280	9	h.	h.	PROPN
eurjchem-267	280	10	n.	n.	PROPN
eurjchem-267	280	11	;	;	PUNCT
eurjchem-267	280	12	nawwar	nawwar	PROPN
eurjchem-267	280	13	,	,	PUNCT
eurjchem-267	280	14	g.	g.	PROPN
eurjchem-267	280	15	a.	a.	PROPN
eurjchem-267	280	16	eur	eur	PROPN
eurjchem-267	280	17	.	.	PUNCT
eurjchem-267	281	1	j.	j.	PROPN
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eurjchem-267	281	3	.	.	PROPN
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eurjchem-267	281	5	.	.	PUNCT
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eurjchem-267	282	2	,	,	PUNCT
eurjchem-267	282	3	44	44	NUM
eurjchem-267	282	4	,	,	PUNCT
eurjchem-267	282	5	1427‐1436	1427‐1436	NUM
eurjchem-267	282	6	.	.	PUNCT
eurjchem-267	283	1	[	[	X
eurjchem-267	283	2	21	21	NUM
eurjchem-267	283	3	]	]	PUNCT
eurjchem-267	283	4	.	.	PUNCT
eurjchem-267	284	1	witt	witt	PROPN
eurjchem-267	284	2	,	,	PUNCT
eurjchem-267	284	3	a.	a.	NOUN
eurjchem-267	284	4	;	;	PUNCT
eurjchem-267	284	5	bergman	bergman	PROPN
eurjchem-267	284	6	,	,	PUNCT
eurjchem-267	284	7	j.	j.	PROPN
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eurjchem-267	284	9	.	.	PUNCT
eurjchem-267	284	10	org	org	PROPN
eurjchem-267	284	11	.	.	PUNCT
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eurjchem-267	284	13	.	.	PUNCT
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eurjchem-267	285	2	,	,	PUNCT
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eurjchem-267	285	4	,	,	PUNCT
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eurjchem-267	285	6	.	.	PUNCT
eurjchem-267	286	1	[	[	X
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eurjchem-267	286	4	.	.	PUNCT
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eurjchem-267	287	2	,	,	PUNCT
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eurjchem-267	287	4	;	;	PUNCT
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eurjchem-267	287	6	,	,	PUNCT
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eurjchem-267	287	9	org	org	PROPN
eurjchem-267	287	10	.	.	PUNCT
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eurjchem-267	287	12	.	.	PUNCT
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eurjchem-267	288	2	,	,	PUNCT
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eurjchem-267	288	4	,	,	PUNCT
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eurjchem-267	288	6	.	.	PUNCT
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eurjchem-267	290	1	[	[	X
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eurjchem-267	290	3	]	]	PUNCT
eurjchem-267	290	4	.	.	PUNCT
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eurjchem-267	291	2	,	,	PUNCT
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eurjchem-267	291	6	.	.	PUNCT
eurjchem-267	292	1	prod	prod	PROPN
eurjchem-267	292	2	.	.	PUNCT
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eurjchem-267	293	2	.	.	PROPN
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eurjchem-267	293	4	,	,	PUNCT
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eurjchem-267	293	6	,	,	PUNCT
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eurjchem-267	293	8	.	.	PUNCT
eurjchem-267	294	1	[	[	X
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eurjchem-267	294	3	]	]	PUNCT
eurjchem-267	294	4	.	.	PUNCT
eurjchem-267	295	1	dandia	dandia	PROPN
eurjchem-267	295	2	,	,	PUNCT
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eurjchem-267	295	6	,	,	PUNCT
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eurjchem-267	295	9	flour	flour	PROPN
eurjchem-267	295	10	.	.	PUNCT
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eurjchem-267	296	2	.	.	PUNCT
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eurjchem-267	297	2	,	,	PUNCT
eurjchem-267	297	3	126	126	NUM
eurjchem-267	297	4	,	,	PUNCT
eurjchem-267	297	5	307‐312	307‐312	NUM
eurjchem-267	297	6	.	.	PUNCT
eurjchem-267	298	1	[	[	X
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eurjchem-267	298	3	]	]	PUNCT
eurjchem-267	298	4	.	.	PUNCT
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eurjchem-267	299	2	,	,	PUNCT
eurjchem-267	299	3	g.	g.	PROPN
eurjchem-267	299	4	;	;	PUNCT
eurjchem-267	299	5	kini	kini	PROPN
eurjchem-267	299	6	,	,	PUNCT
eurjchem-267	299	7	s.	s.	PROPN
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eurjchem-267	299	10	.	.	PUNCT
eurjchem-267	300	1	j.	j.	PROPN
eurjchem-267	300	2	med	med	PROPN
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eurjchem-267	300	5	.	.	PUNCT
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eurjchem-267	301	2	,	,	PUNCT
eurjchem-267	301	3	41	41	NUM
eurjchem-267	301	4	,	,	PUNCT
eurjchem-267	301	5	256‐262	256‐262	NUM
eurjchem-267	301	6	.	.	PUNCT
eurjchem-267	302	1	[	[	X
eurjchem-267	302	2	26	26	NUM
eurjchem-267	302	3	]	]	PUNCT
eurjchem-267	302	4	.	.	PUNCT
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eurjchem-267	303	2	,	,	PUNCT
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eurjchem-267	303	5	;	;	PUNCT
eurjchem-267	303	6	reddy	reddy	PROPN
eurjchem-267	303	7	,	,	PUNCT
eurjchem-267	303	8	p.	p.	PROPN
eurjchem-267	303	9	p.	p.	PROPN
eurjchem-267	303	10	;	;	PUNCT
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eurjchem-267	303	12	,	,	PUNCT
eurjchem-267	303	13	t.	t.	NOUN
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eurjchem-267	303	16	,	,	PUNCT
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eurjchem-267	303	18	,	,	PUNCT
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eurjchem-267	303	20	.	.	PUNCT
eurjchem-267	304	1	[	[	X
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eurjchem-267	304	3	]	]	PUNCT
eurjchem-267	304	4	.	.	PUNCT
eurjchem-267	305	1	kumar	kumar	PROPN
eurjchem-267	305	2	,	,	PUNCT
eurjchem-267	305	3	v.	v.	PROPN
eurjchem-267	305	4	;	;	PUNCT
eurjchem-267	305	5	mohan	mohan	PROPN
eurjchem-267	305	6	,	,	PUNCT
eurjchem-267	305	7	c.	c.	PROPN
eurjchem-267	305	8	;	;	PUNCT
eurjchem-267	305	9	mahajan	mahajan	PROPN
eurjchem-267	305	10	,	,	PUNCT
eurjchem-267	305	11	m.	m.	NOUN
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eurjchem-267	305	15	,	,	PUNCT
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eurjchem-267	305	17	,	,	PUNCT
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eurjchem-267	305	20	.	.	PUNCT
eurjchem-267	306	1	[	[	X
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eurjchem-267	306	3	]	]	PUNCT
eurjchem-267	306	4	.	.	PUNCT
eurjchem-267	307	1	mahmoud	mahmoud	PROPN
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eurjchem-267	309	2	,	,	PUNCT
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eurjchem-267	309	4	,	,	PUNCT
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eurjchem-267	309	7	.	.	PUNCT
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eurjchem-267	310	3	]	]	PUNCT
eurjchem-267	310	4	.	.	PUNCT
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eurjchem-267	311	2	,	,	PUNCT
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eurjchem-267	311	7	,	,	PUNCT
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eurjchem-267	311	17	.	.	PUNCT
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eurjchem-267	312	2	.	.	PUNCT
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eurjchem-267	313	2	,	,	PUNCT
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eurjchem-267	313	4	)	)	PUNCT
eurjchem-267	313	5	,	,	PUNCT
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eurjchem-267	314	3	.	.	PUNCT
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eurjchem-267	315	3	]	]	PUNCT
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eurjchem-267	316	2	,	,	PUNCT
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eurjchem-267	316	19	.	.	PUNCT
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eurjchem-267	317	2	,	,	PUNCT
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eurjchem-267	317	4	)	)	PUNCT
eurjchem-267	317	5	,	,	PUNCT
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eurjchem-267	317	7	.	.	PUNCT
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eurjchem-267	318	3	]	]	PUNCT
eurjchem-267	318	4	.	.	PUNCT
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eurjchem-267	319	2	,	,	PUNCT
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eurjchem-267	319	4	;	;	PUNCT
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eurjchem-267	319	6	,	,	PUNCT
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eurjchem-267	319	8	;	;	PUNCT
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eurjchem-267	319	10	,	,	PUNCT
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eurjchem-267	319	22	lett	lett	PROPN
eurjchem-267	319	23	.	.	PUNCT
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eurjchem-267	320	2	,	,	PUNCT
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eurjchem-267	320	4	)	)	PUNCT
eurjchem-267	320	5	,	,	PUNCT
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eurjchem-267	321	2	.	.	PUNCT
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eurjchem-267	322	3	]	]	PUNCT
eurjchem-267	322	4	.	.	PUNCT
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eurjchem-267	323	2	,	,	PUNCT
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eurjchem-267	323	4	;	;	PUNCT
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eurjchem-267	323	15	,	,	PUNCT
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eurjchem-267	324	28	.	.	PUNCT
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eurjchem-267	325	7	,	,	PUNCT
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eurjchem-267	325	27	.	.	PUNCT
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eurjchem-267	326	2	.	.	PROPN
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eurjchem-267	326	4	,	,	PUNCT
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eurjchem-267	326	8	.	.	PUNCT
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eurjchem-267	327	3	]	]	PUNCT
eurjchem-267	327	4	.	.	PUNCT
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eurjchem-267	328	2	,	,	PUNCT
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eurjchem-267	330	3	]	]	PUNCT
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eurjchem-267	332	3	.	.	PUNCT
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eurjchem-267	333	2	,	,	PUNCT
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eurjchem-267	333	4	,	,	PUNCT
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eurjchem-267	334	4	.	.	PUNCT
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eurjchem-267	335	7	,	,	PUNCT
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eurjchem-267	335	24	.	.	PUNCT
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eurjchem-267	336	2	,	,	PUNCT
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eurjchem-267	336	4	,	,	PUNCT
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eurjchem-267	336	6	.	.	PUNCT
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eurjchem-267	337	4	.	.	PUNCT
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eurjchem-267	338	5	;	;	PUNCT
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eurjchem-267	339	2	.	.	PROPN
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eurjchem-267	339	4	,	,	PUNCT
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eurjchem-267	339	6	,	,	PUNCT
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eurjchem-267	339	8	.	.	PUNCT
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eurjchem-267	340	3	]	]	PUNCT
eurjchem-267	340	4	.	.	PUNCT
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eurjchem-267	341	5	;	;	PUNCT
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eurjchem-267	341	24	.	.	PUNCT
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eurjchem-267	342	2	.	.	PUNCT
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eurjchem-267	343	2	,	,	PUNCT
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eurjchem-267	343	4	,	,	PUNCT
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eurjchem-267	343	6	.	.	PUNCT
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eurjchem-267	344	4	.	.	PUNCT
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eurjchem-267	345	24	.	.	PUNCT
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eurjchem-267	346	3	.	.	PUNCT
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eurjchem-267	347	2	,	,	PUNCT
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eurjchem-267	347	4	)	)	PUNCT
eurjchem-267	347	5	,	,	PUNCT
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