id	sid	tid	token	lemma	pos
eurjchem-289	1	1	untitled	untitle	VERB
eurjchem-289	1	2	european	european	PROPN
eurjchem-289	1	3	journal	journal	PROPN
eurjchem-289	1	4	of	of	ADP
eurjchem-289	1	5	chemistry	chemistry	NOUN
eurjchem-289	1	6	2	2	NUM
eurjchem-289	1	7	(	(	PUNCT
eurjchem-289	1	8	3	3	NUM
eurjchem-289	1	9	)	)	PUNCT
eurjchem-289	1	10	(	(	PUNCT
eurjchem-289	1	11	2011	2011	NUM
eurjchem-289	1	12	)	)	PUNCT
eurjchem-289	1	13	365‐371	365‐371	PROPN
eurjchem-289	1	14	european	european	PROPN
eurjchem-289	1	15	journal	journal	PROPN
eurjchem-289	1	16	of	of	ADP
eurjchem-289	1	17	chemistry	chemistry	NOUN
eurjchem-289	1	18	issn	issn	PROPN
eurjchem-289	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-289	1	20	(	(	PUNCT
eurjchem-289	1	21	print	print	NOUN
eurjchem-289	1	22	)	)	PUNCT
eurjchem-289	1	23	/	/	SYM
eurjchem-289	1	24	issn	issn	PROPN
eurjchem-289	1	25	2153‐2257	2153‐2257	NUM
eurjchem-289	1	26	(	(	PUNCT
eurjchem-289	1	27	online	online	ADJ
eurjchem-289	1	28	)	)	PUNCT
eurjchem-289	1	29			NOUN
eurjchem-289	1	30	2011	2011	NUM
eurjchem-289	1	31	eurjchem	eurjchem	PROPN
eurjchem-289	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-289	1	33	/	/	SYM
eurjchem-289	1	34	eurjchem.2.3.365‐371.289	eurjchem.2.3.365‐371.289	ADJ
eurjchem-289	1	35	european	european	ADJ
eurjchem-289	1	36	journal	journal	PROPN
eurjchem-289	1	37	of	of	ADP
eurjchem-289	1	38	chemistry	chemistry	PROPN
eurjchem-289	1	39	journal	journal	PROPN
eurjchem-289	1	40	homepage	homepage	NOUN
eurjchem-289	1	41	:	:	PUNCT
eurjchem-289	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-289	1	43	synthesis	synthesis	NOUN
eurjchem-289	1	44	of	of	ADP
eurjchem-289	1	45	novel	novel	NOUN
eurjchem-289	1	46	3,4‐dihydroquinoxalin‐2(1h)‐one	3,4‐dihydroquinoxalin‐2(1h)‐one	NUM
eurjchem-289	1	47	derivatives	derivative	NOUN
eurjchem-289	1	48	mohammed	mohammed	PROPN
eurjchem-289	1	49	shabaan	shabaan	PROPN
eurjchem-289	1	50	,	,	PUNCT
eurjchem-289	1	51	azza	azza	VERB
eurjchem-289	1	52	taher	taher	PROPN
eurjchem-289	1	53	taher	taher	PROPN
eurjchem-289	1	54	*	*	PUNCT
eurjchem-289	1	55	and	and	CCONJ
eurjchem-289	1	56	eman	eman	PROPN
eurjchem-289	1	57	omar	omar	PROPN
eurjchem-289	1	58	osman	osman	PROPN
eurjchem-289	1	59	department	department	PROPN
eurjchem-289	1	60	of	of	ADP
eurjchem-289	1	61	organic	organic	ADJ
eurjchem-289	1	62	chemistry	chemistry	NOUN
eurjchem-289	1	63	,	,	PUNCT
eurjchem-289	1	64	faculty	faculty	NOUN
eurjchem-289	1	65	of	of	ADP
eurjchem-289	1	66	pharmacy	pharmacy	NOUN
eurjchem-289	1	67	,	,	PUNCT
eurjchem-289	1	68	cairo	cairo	PROPN
eurjchem-289	1	69	university	university	PROPN
eurjchem-289	1	70	,	,	PUNCT
eurjchem-289	1	71	cairo	cairo	PROPN
eurjchem-289	1	72	,	,	PUNCT
eurjchem-289	1	73	11562	11562	NUM
eurjchem-289	1	74	,	,	PUNCT
eurjchem-289	1	75	egypt	egypt	PROPN
eurjchem-289	1	76	*	*	PUNCT
eurjchem-289	1	77	corresponding	correspond	VERB
eurjchem-289	1	78	author	author	NOUN
eurjchem-289	1	79	at	at	ADP
eurjchem-289	1	80	:	:	PUNCT
eurjchem-289	1	81	department	department	NOUN
eurjchem-289	1	82	of	of	ADP
eurjchem-289	1	83	organic	organic	ADJ
eurjchem-289	1	84	chemistry	chemistry	NOUN
eurjchem-289	1	85	,	,	PUNCT
eurjchem-289	1	86	faculty	faculty	NOUN
eurjchem-289	1	87	of	of	ADP
eurjchem-289	1	88	pharmacy	pharmacy	NOUN
eurjchem-289	1	89	,	,	PUNCT
eurjchem-289	1	90	cairo	cairo	PROPN
eurjchem-289	1	91	university	university	PROPN
eurjchem-289	1	92	,	,	PUNCT
eurjchem-289	1	93	cairo	cairo	PROPN
eurjchem-289	1	94	,	,	PUNCT
eurjchem-289	1	95	11562	11562	NUM
eurjchem-289	1	96	,	,	PUNCT
eurjchem-289	1	97	egypt	egypt	PROPN
eurjchem-289	1	98	.	.	PUNCT
eurjchem-289	2	1	tel	tel	PROPN
eurjchem-289	2	2	.	.	PUNCT
eurjchem-289	2	3	:	:	PUNCT
eurjchem-289	3	1	+2.0101470792	+2.0101470792	ADV
eurjchem-289	3	2	;	;	PUNCT
eurjchem-289	3	3	fax	fax	NOUN
eurjchem-289	3	4	:	:	PUNCT
eurjchem-289	3	5	+2.023639307	+2.023639307	NUM
eurjchem-289	3	6	.	.	PUNCT
eurjchem-289	3	7	e‐mail	e‐mail	PUNCT
eurjchem-289	4	1	address	address	NOUN
eurjchem-289	4	2	:	:	PUNCT
eurjchem-289	4	3	azzataher2005@yahoo.com	azzataher2005@yahoo.com	X
eurjchem-289	4	4	(	(	PUNCT
eurjchem-289	4	5	a.t	a.t	PROPN
eurjchem-289	4	6	.	.	PROPN
eurjchem-289	4	7	taher	taher	PROPN
eurjchem-289	4	8	)	)	PUNCT
eurjchem-289	4	9	.	.	PUNCT
eurjchem-289	5	1	article	article	NOUN
eurjchem-289	5	2	information	information	PROPN
eurjchem-289	5	3	abstract	abstract	ADV
eurjchem-289	5	4	received	receive	VERB
eurjchem-289	5	5	:	:	PUNCT
eurjchem-289	5	6	27	27	NUM
eurjchem-289	5	7	october	october	NOUN
eurjchem-289	5	8	2010	2010	NUM
eurjchem-289	5	9	received	receive	VERB
eurjchem-289	5	10	in	in	ADP
eurjchem-289	5	11	revised	revise	VERB
eurjchem-289	5	12	form	form	NOUN
eurjchem-289	5	13	:	:	PUNCT
eurjchem-289	5	14	22	22	NUM
eurjchem-289	5	15	december	december	PROPN
eurjchem-289	5	16	2010	2010	NUM
eurjchem-289	5	17	accepted	accept	VERB
eurjchem-289	5	18	:	:	PUNCT
eurjchem-289	5	19	24	24	NUM
eurjchem-289	5	20	december	december	PROPN
eurjchem-289	5	21	2010	2010	NUM
eurjchem-289	5	22	online	online	NOUN
eurjchem-289	5	23	:	:	PUNCT
eurjchem-289	5	24	30	30	NUM
eurjchem-289	5	25	september	september	PROPN
eurjchem-289	5	26	2011	2011	NUM
eurjchem-289	5	27	keywords	keyword	VERB
eurjchem-289	5	28	new	new	ADJ
eurjchem-289	5	29	derivatives	derivative	NOUN
eurjchem-289	5	30	of	of	ADP
eurjchem-289	5	31	3,4‐dihydroquinoxaline‐2(1h)‐one	3,4‐dihydroquinoxaline‐2(1h)‐one	NUM
eurjchem-289	5	32	were	be	AUX
eurjchem-289	5	33	synthesized	synthesize	VERB
eurjchem-289	5	34	and	and	CCONJ
eurjchem-289	5	35	characterized	characterize	VERB
eurjchem-289	5	36	.	.	PUNCT
eurjchem-289	6	1	representative	representative	ADJ
eurjchem-289	6	2	examples	example	NOUN
eurjchem-289	6	3	were	be	AUX
eurjchem-289	6	4	evaluated	evaluate	VERB
eurjchem-289	6	5	for	for	ADP
eurjchem-289	6	6	their	their	PRON
eurjchem-289	6	7	antimicrobial	antimicrobial	ADJ
eurjchem-289	6	8	and	and	CCONJ
eurjchem-289	6	9	antifungal	antifungal	ADJ
eurjchem-289	6	10	activities	activity	NOUN
eurjchem-289	6	11	using	use	VERB
eurjchem-289	6	12	tetracycline	tetracycline	NOUN
eurjchem-289	6	13	and	and	CCONJ
eurjchem-289	6	14	nystatin	nystatin	NOUN
eurjchem-289	6	15	as	as	ADP
eurjchem-289	6	16	reference	reference	NOUN
eurjchem-289	6	17	compound	compound	NOUN
eurjchem-289	6	18	.	.	PUNCT
eurjchem-289	7	1	one	one	NUM
eurjchem-289	7	2	of	of	ADP
eurjchem-289	7	3	the	the	DET
eurjchem-289	7	4	tested	test	VERB
eurjchem-289	7	5	compounds	compound	NOUN
eurjchem-289	7	6	10a	10a	NOUN
eurjchem-289	7	7	was	be	AUX
eurjchem-289	7	8	found	find	VERB
eurjchem-289	7	9	to	to	PART
eurjchem-289	7	10	exhibit	exhibit	VERB
eurjchem-289	7	11	slight	slight	ADJ
eurjchem-289	7	12	activity	activity	NOUN
eurjchem-289	7	13	against	against	ADP
eurjchem-289	7	14	staphylococcus	staphylococcus	NOUN
eurjchem-289	7	15	aureus	aureus	NOUN
eurjchem-289	7	16	.	.	PUNCT
eurjchem-289	8	1	compounds	compound	VERB
eurjchem-289	8	2	10b	10b	NOUN
eurjchem-289	8	3	,	,	PUNCT
eurjchem-289	8	4	11b	11b	NOUN
eurjchem-289	8	5	and	and	CCONJ
eurjchem-289	8	6	14b	14b	NUM
eurjchem-289	8	7	showed	show	VERB
eurjchem-289	8	8	slight	slight	ADJ
eurjchem-289	8	9	activity	activity	NOUN
eurjchem-289	8	10	against	against	ADP
eurjchem-289	8	11	escherichia	escherichia	NOUN
eurjchem-289	8	12	coli	coli	NOUN
eurjchem-289	8	13	.	.	PUNCT
eurjchem-289	9	1	moreover	moreover	ADV
eurjchem-289	9	2	,	,	PUNCT
eurjchem-289	9	3	nineteen	nineteen	NUM
eurjchem-289	9	4	compounds	compound	NOUN
eurjchem-289	9	5	were	be	AUX
eurjchem-289	9	6	screened	screen	VERB
eurjchem-289	9	7	for	for	ADP
eurjchem-289	9	8	their	their	PRON
eurjchem-289	9	9	inhibition	inhibition	NOUN
eurjchem-289	9	10	effect	effect	NOUN
eurjchem-289	9	11	on	on	ADP
eurjchem-289	9	12	cdk5	cdk5	PROPN
eurjchem-289	9	13	,	,	PUNCT
eurjchem-289	9	14	ck1	ck1	PROPN
eurjchem-289	9	15	,	,	PUNCT
eurjchem-289	9	16	and	and	CCONJ
eurjchem-289	9	17	gsk‐3β	gsk‐3β	PROPN
eurjchem-289	9	18	.	.	PUNCT
eurjchem-289	10	1	none	none	NOUN
eurjchem-289	10	2	of	of	ADP
eurjchem-289	10	3	the	the	DET
eurjchem-289	10	4	tested	test	VERB
eurjchem-289	10	5	compounds	compound	NOUN
eurjchem-289	10	6	showed	show	VERB
eurjchem-289	10	7	an	an	DET
eurjchem-289	10	8	inhibition	inhibition	NOUN
eurjchem-289	10	9	activity	activity	NOUN
eurjchem-289	10	10	below	below	ADP
eurjchem-289	10	11	10	10	NUM
eurjchem-289	10	12	µm	µm	ADP
eurjchem-289	10	13	concentration	concentration	NOUN
eurjchem-289	10	14	.	.	PUNCT
eurjchem-289	11	1	quinoxaline	quinoxaline	PROPN
eurjchem-289	11	2	3,4‐dihydroquinoxalin	3,4‐dihydroquinoxalin	DET
eurjchem-289	11	3	antimicrobial	antimicrobial	ADJ
eurjchem-289	11	4	activity	activity	NOUN
eurjchem-289	11	5	ck1	ck1	NOUN
eurjchem-289	11	6	inhibitors	inhibitor	NOUN
eurjchem-289	11	7	cdk5	cdk5	VERB
eurjchem-289	11	8	inhibitors	inhibitor	NOUN
eurjchem-289	11	9	gsk‐3β	gsk‐3β	VERB
eurjchem-289	11	10	inhibitors	inhibitor	NOUN
eurjchem-289	11	11	1	1	NUM
eurjchem-289	11	12	.	.	PUNCT
eurjchem-289	12	1	introduction	introduction	NOUN
eurjchem-289	12	2	quinoxaline	quinoxaline	PROPN
eurjchem-289	12	3	ring	ring	NOUN
eurjchem-289	12	4	system	system	NOUN
eurjchem-289	12	5	represents	represent	VERB
eurjchem-289	12	6	the	the	DET
eurjchem-289	12	7	building	building	NOUN
eurjchem-289	12	8	block	block	NOUN
eurjchem-289	12	9	of	of	ADP
eurjchem-289	12	10	many	many	ADJ
eurjchem-289	12	11	biologically	biologically	ADV
eurjchem-289	12	12	active	active	ADJ
eurjchem-289	12	13	compounds	compound	NOUN
eurjchem-289	12	14	that	that	PRON
eurjchem-289	12	15	possess	possess	VERB
eurjchem-289	12	16	anti‐	anti‐	NOUN
eurjchem-289	12	17	inflammatory	inflammatory	ADJ
eurjchem-289	12	18	[	[	X
eurjchem-289	12	19	1,2	1,2	NUM
eurjchem-289	12	20	]	]	PUNCT
eurjchem-289	12	21	,	,	PUNCT
eurjchem-289	12	22	antibacterial	antibacterial	ADJ
eurjchem-289	12	23	[	[	X
eurjchem-289	12	24	3‐5	3‐5	NUM
eurjchem-289	12	25	]	]	PUNCT
eurjchem-289	12	26	,	,	PUNCT
eurjchem-289	12	27	antifungal	antifungal	PROPN
eurjchem-289	13	1	[	[	X
eurjchem-289	13	2	6	6	NUM
eurjchem-289	13	3	]	]	PUNCT
eurjchem-289	13	4	,	,	PUNCT
eurjchem-289	13	5	anticancer	anticancer	NOUN
eurjchem-289	14	1	[	[	X
eurjchem-289	14	2	7,8	7,8	NUM
eurjchem-289	14	3	]	]	PUNCT
eurjchem-289	14	4	,	,	PUNCT
eurjchem-289	14	5	antimalarial	antimalarial	ADJ
eurjchem-289	14	6	[	[	X
eurjchem-289	14	7	9	9	NUM
eurjchem-289	14	8	]	]	PUNCT
eurjchem-289	14	9	,	,	PUNCT
eurjchem-289	14	10	cns	cns	PROPN
eurjchem-289	14	11	depressant	depressant	NOUN
eurjchem-289	14	12	[	[	X
eurjchem-289	14	13	10	10	NUM
eurjchem-289	14	14	]	]	PUNCT
eurjchem-289	14	15	and	and	CCONJ
eurjchem-289	14	16	hypoglycemic	hypoglycemic	ADJ
eurjchem-289	14	17	[	[	X
eurjchem-289	14	18	11	11	NUM
eurjchem-289	14	19	]	]	PUNCT
eurjchem-289	14	20	activities	activity	NOUN
eurjchem-289	14	21	.	.	PUNCT
eurjchem-289	15	1	cyclin‐dependent	cyclin‐dependent	PROPN
eurjchem-289	15	2	kinase	kinase	PROPN
eurjchem-289	15	3	5	5	NUM
eurjchem-289	15	4	(	(	PUNCT
eurjchem-289	15	5	cdk5	cdk5	PROPN
eurjchem-289	15	6	)	)	PUNCT
eurjchem-289	15	7	is	be	AUX
eurjchem-289	15	8	a	a	DET
eurjchem-289	15	9	protein	protein	NOUN
eurjchem-289	15	10	kinase	kinase	NOUN
eurjchem-289	15	11	believed	believe	VERB
eurjchem-289	15	12	to	to	PART
eurjchem-289	15	13	play	play	VERB
eurjchem-289	15	14	a	a	DET
eurjchem-289	15	15	critical	critical	ADJ
eurjchem-289	15	16	role	role	NOUN
eurjchem-289	15	17	in	in	ADP
eurjchem-289	15	18	the	the	DET
eurjchem-289	15	19	early	early	ADJ
eurjchem-289	15	20	development	development	NOUN
eurjchem-289	15	21	of	of	ADP
eurjchem-289	15	22	the	the	DET
eurjchem-289	15	23	central	central	ADJ
eurjchem-289	15	24	nervous	nervous	ADJ
eurjchem-289	15	25	system	system	NOUN
eurjchem-289	15	26	[	[	X
eurjchem-289	15	27	12,13	12,13	NUM
eurjchem-289	15	28	]	]	PUNCT
eurjchem-289	15	29	.	.	PUNCT
eurjchem-289	16	1	it	it	PRON
eurjchem-289	16	2	is	be	AUX
eurjchem-289	16	3	shown	show	VERB
eurjchem-289	16	4	to	to	PART
eurjchem-289	16	5	be	be	AUX
eurjchem-289	16	6	involved	involve	VERB
eurjchem-289	16	7	in	in	ADP
eurjchem-289	16	8	cellular	cellular	ADJ
eurjchem-289	16	9	processes	process	NOUN
eurjchem-289	16	10	like	like	ADP
eurjchem-289	16	11	neuronal	neuronal	ADJ
eurjchem-289	16	12	differentiation	differentiation	NOUN
eurjchem-289	16	13	[	[	X
eurjchem-289	16	14	14	14	NUM
eurjchem-289	16	15	]	]	PUNCT
eurjchem-289	16	16	,	,	PUNCT
eurjchem-289	16	17	cell	cell	NOUN
eurjchem-289	16	18	adhesion	adhesion	NOUN
eurjchem-289	16	19	[	[	X
eurjchem-289	16	20	15	15	NUM
eurjchem-289	16	21	]	]	PUNCT
eurjchem-289	16	22	,	,	PUNCT
eurjchem-289	16	23	and	and	CCONJ
eurjchem-289	16	24	axonal	axonal	ADJ
eurjchem-289	16	25	guidance	guidance	NOUN
eurjchem-289	16	26	[	[	X
eurjchem-289	16	27	16	16	NUM
eurjchem-289	16	28	]	]	PUNCT
eurjchem-289	16	29	.	.	PUNCT
eurjchem-289	17	1	recently	recently	ADV
eurjchem-289	17	2	,	,	PUNCT
eurjchem-289	17	3	a	a	DET
eurjchem-289	17	4	large	large	ADJ
eurjchem-289	17	5	body	body	NOUN
eurjchem-289	17	6	of	of	ADP
eurjchem-289	17	7	evidence	evidence	NOUN
eurjchem-289	17	8	suggests	suggest	VERB
eurjchem-289	17	9	that	that	SCONJ
eurjchem-289	17	10	deregulation	deregulation	NOUN
eurjchem-289	17	11	of	of	ADP
eurjchem-289	17	12	cdk5	cdk5	PROPN
eurjchem-289	17	13	is	be	AUX
eurjchem-289	17	14	implicated	implicate	VERB
eurjchem-289	17	15	in	in	ADP
eurjchem-289	17	16	the	the	DET
eurjchem-289	17	17	pathology	pathology	NOUN
eurjchem-289	17	18	of	of	ADP
eurjchem-289	17	19	a	a	DET
eurjchem-289	17	20	number	number	NOUN
eurjchem-289	17	21	of	of	ADP
eurjchem-289	17	22	neurodegenerative	neurodegenerative	ADJ
eurjchem-289	17	23	disorders	disorder	NOUN
eurjchem-289	17	24	.	.	PUNCT
eurjchem-289	18	1	as	as	ADP
eurjchem-289	18	2	a	a	DET
eurjchem-289	18	3	consequence	consequence	NOUN
eurjchem-289	18	4	,	,	PUNCT
eurjchem-289	18	5	cdk5	cdk5	PROPN
eurjchem-289	18	6	inhibitors	inhibitor	NOUN
eurjchem-289	18	7	are	be	AUX
eurjchem-289	18	8	of	of	ADP
eurjchem-289	18	9	potential	potential	ADJ
eurjchem-289	18	10	therapeutic	therapeutic	ADJ
eurjchem-289	18	11	uses	use	NOUN
eurjchem-289	18	12	for	for	ADP
eurjchem-289	18	13	diseases	disease	NOUN
eurjchem-289	18	14	such	such	ADJ
eurjchem-289	18	15	as	as	ADP
eurjchem-289	18	16	alzheimer	alzheimer	NOUN
eurjchem-289	18	17	's	's	PART
eurjchem-289	18	18	disease	disease	NOUN
eurjchem-289	18	19	[	[	X
eurjchem-289	18	20	17	17	NUM
eurjchem-289	18	21	]	]	PUNCT
eurjchem-289	18	22	,	,	PUNCT
eurjchem-289	18	23	parkinson	parkinson	NOUN
eurjchem-289	18	24	's	's	PART
eurjchem-289	18	25	disease	disease	NOUN
eurjchem-289	18	26	[	[	X
eurjchem-289	18	27	18	18	NUM
eurjchem-289	18	28	]	]	PUNCT
eurjchem-289	18	29	,	,	PUNCT
eurjchem-289	18	30	amyotrophic	amyotrophic	ADJ
eurjchem-289	18	31	lateral	lateral	ADJ
eurjchem-289	18	32	sclerosis	sclerosis	NOUN
eurjchem-289	19	1	[	[	X
eurjchem-289	19	2	19	19	NUM
eurjchem-289	19	3	]	]	PUNCT
eurjchem-289	19	4	and	and	CCONJ
eurjchem-289	19	5	ischemic	ischemic	ADJ
eurjchem-289	19	6	stroke	stroke	NOUN
eurjchem-289	19	7	[	[	X
eurjchem-289	19	8	20	20	NUM
eurjchem-289	19	9	]	]	PUNCT
eurjchem-289	19	10	.	.	PUNCT
eurjchem-289	20	1	from	from	ADP
eurjchem-289	20	2	high	high	ADJ
eurjchem-289	20	3	throughput	throughput	NOUN
eurjchem-289	20	4	screening	screen	VERB
eurjchem-289	20	5	efforts	effort	NOUN
eurjchem-289	20	6	,	,	PUNCT
eurjchem-289	20	7	we	we	PRON
eurjchem-289	20	8	identified	identify	VERB
eurjchem-289	20	9	the	the	DET
eurjchem-289	20	10	structure	structure	NOUN
eurjchem-289	20	11	activity	activity	NOUN
eurjchem-289	20	12	relationship	relationship	NOUN
eurjchem-289	20	13	of	of	ADP
eurjchem-289	20	14	potent	potent	ADJ
eurjchem-289	20	15	cdk2	cdk2	NOUN
eurjchem-289	20	16	and	and	CCONJ
eurjchem-289	20	17	cdk5	cdk5	PROPN
eurjchem-289	20	18	inhibitors	inhibitor	NOUN
eurjchem-289	20	19	based	base	VERB
eurjchem-289	20	20	on	on	ADP
eurjchem-289	20	21	five	five	NUM
eurjchem-289	20	22	member	member	NOUN
eurjchem-289	20	23	ring	ring	NOUN
eurjchem-289	20	24	attached	attach	VERB
eurjchem-289	20	25	to	to	ADP
eurjchem-289	20	26	quinoline‐	quinoline‐	PROPN
eurjchem-289	20	27	2(1h)‐one	2(1h)‐one	NUM
eurjchem-289	20	28	,	,	PUNCT
eurjchem-289	20	29	or	or	CCONJ
eurjchem-289	20	30	3,4‐dihyro‐1h‐quinazoline‐2‐ones	3,4‐dihyro‐1h‐quinazoline‐2‐ones	NUM
eurjchem-289	20	31	[	[	X
eurjchem-289	20	32	21,22	21,22	X
eurjchem-289	20	33	]	]	X
eurjchem-289	20	34	.	.	PUNCT
eurjchem-289	21	1	in	in	ADP
eurjchem-289	21	2	our	our	PRON
eurjchem-289	21	3	efforts	effort	NOUN
eurjchem-289	21	4	to	to	PART
eurjchem-289	21	5	discover	discover	VERB
eurjchem-289	21	6	more	more	ADV
eurjchem-289	21	7	potent	potent	ADJ
eurjchem-289	21	8	inhibitors	inhibitor	NOUN
eurjchem-289	21	9	and	and	CCONJ
eurjchem-289	21	10	an	an	DET
eurjchem-289	21	11	extension	extension	NOUN
eurjchem-289	21	12	of	of	ADP
eurjchem-289	21	13	these	these	DET
eurjchem-289	21	14	studies	study	NOUN
eurjchem-289	21	15	we	we	PRON
eurjchem-289	21	16	introduced	introduce	VERB
eurjchem-289	21	17	some	some	DET
eurjchem-289	21	18	modification	modification	NOUN
eurjchem-289	21	19	,	,	PUNCT
eurjchem-289	21	20	firstly	firstly	ADV
eurjchem-289	21	21	the	the	DET
eurjchem-289	21	22	designed	design	VERB
eurjchem-289	21	23	compounds	compound	NOUN
eurjchem-289	21	24	included	include	VERB
eurjchem-289	21	25	fusion	fusion	NOUN
eurjchem-289	21	26	of	of	ADP
eurjchem-289	21	27	quinoxaline	quinoxaline	ADJ
eurjchem-289	21	28	ring	ring	NOUN
eurjchem-289	21	29	either	either	CCONJ
eurjchem-289	21	30	with	with	ADP
eurjchem-289	21	31	six	six	NUM
eurjchem-289	21	32	member	member	NOUN
eurjchem-289	21	33	pyridinone	pyridinone	NOUN
eurjchem-289	21	34	ring	ring	NOUN
eurjchem-289	21	35	compound	compound	NOUN
eurjchem-289	21	36	4	4	NUM
eurjchem-289	21	37	or	or	CCONJ
eurjchem-289	21	38	five	five	NUM
eurjchem-289	21	39	member	member	NOUN
eurjchem-289	21	40	furan	furan	PROPN
eurjchem-289	21	41	ring	ring	NOUN
eurjchem-289	21	42	compounds	compound	VERB
eurjchem-289	21	43	9a‐c	9a‐c	PROPN
eurjchem-289	21	44	.	.	PUNCT
eurjchem-289	22	1	secondly	secondly	ADV
eurjchem-289	22	2	,	,	PUNCT
eurjchem-289	22	3	quinoxaline‐2(1h)‐ones	quinoxaline‐2(1h)‐one	NOUN
eurjchem-289	22	4	were	be	AUX
eurjchem-289	22	5	linked	link	VERB
eurjchem-289	22	6	either	either	CCONJ
eurjchem-289	22	7	to	to	ADP
eurjchem-289	22	8	3‐aryl‐six	3‐aryl‐six	NUM
eurjchem-289	22	9	member	member	NOUN
eurjchem-289	22	10	ring	ring	NOUN
eurjchem-289	22	11	compounds	compound	VERB
eurjchem-289	22	12	5	5	NUM
eurjchem-289	22	13	,	,	PUNCT
eurjchem-289	22	14	6a‐	6a‐	NUM
eurjchem-289	22	15	c	c	NOUN
eurjchem-289	22	16	or	or	CCONJ
eurjchem-289	22	17	3‐aryl‐five	3‐aryl‐five	NUM
eurjchem-289	22	18	member	member	NOUN
eurjchem-289	22	19	ring	ring	NOUN
eurjchem-289	22	20	via	via	ADP
eurjchem-289	22	21	methylene	methylene	NOUN
eurjchem-289	22	22	spacer	spacer	NOUN
eurjchem-289	22	23	compounds	compound	VERB
eurjchem-289	22	24	10a	10a	NOUN
eurjchem-289	22	25	,	,	PUNCT
eurjchem-289	22	26	b	b	PROPN
eurjchem-289	22	27	(	(	PUNCT
eurjchem-289	22	28	scheme	scheme	NOUN
eurjchem-289	22	29	1	1	NUM
eurjchem-289	22	30	)	)	PUNCT
eurjchem-289	22	31	.	.	PUNCT
eurjchem-289	23	1	in	in	ADP
eurjchem-289	23	2	scheme	scheme	NOUN
eurjchem-289	23	3	2	2	NUM
eurjchem-289	23	4	,	,	PUNCT
eurjchem-289	23	5	quinoxaline‐2(1h)‐ones	quinoxaline‐2(1h)‐one	NOUN
eurjchem-289	23	6	ring	ring	NOUN
eurjchem-289	23	7	is	be	AUX
eurjchem-289	23	8	linked	link	VERB
eurjchem-289	23	9	directly	directly	ADV
eurjchem-289	23	10	either	either	CCONJ
eurjchem-289	23	11	to	to	ADP
eurjchem-289	23	12	phenylpyrazole	phenylpyrazole	ADJ
eurjchem-289	23	13	compound	compound	VERB
eurjchem-289	23	14	12	12	NUM
eurjchem-289	23	15	,	,	PUNCT
eurjchem-289	23	16	or	or	CCONJ
eurjchem-289	23	17	aryloxazine	aryloxazine	NOUN
eurjchem-289	23	18	compounds	compound	NOUN
eurjchem-289	23	19	14a	14a	NOUN
eurjchem-289	23	20	,	,	PUNCT
eurjchem-289	23	21	b.	b.	NOUN
eurjchem-289	24	1	the	the	DET
eurjchem-289	24	2	derivatives	derivative	NOUN
eurjchem-289	24	3	prepared	prepare	VERB
eurjchem-289	24	4	in	in	ADP
eurjchem-289	24	5	this	this	DET
eurjchem-289	24	6	study	study	NOUN
eurjchem-289	24	7	were	be	AUX
eurjchem-289	24	8	evaluated	evaluate	VERB
eurjchem-289	24	9	for	for	ADP
eurjchem-289	24	10	their	their	PRON
eurjchem-289	24	11	ability	ability	NOUN
eurjchem-289	24	12	to	to	PART
eurjchem-289	24	13	inhibit	inhibit	VERB
eurjchem-289	24	14	purified	purify	VERB
eurjchem-289	24	15	human	human	ADJ
eurjchem-289	24	16	cdk	cdk	PROPN
eurjchem-289	24	17	and	and	CCONJ
eurjchem-289	24	18	the	the	DET
eurjchem-289	24	19	ic50	ic50	PROPN
eurjchem-289	24	20	values	value	NOUN
eurjchem-289	24	21	were	be	AUX
eurjchem-289	24	22	reported	report	VERB
eurjchem-289	24	23	in	in	ADP
eurjchem-289	24	24	table	table	NOUN
eurjchem-289	24	25	1	1	NUM
eurjchem-289	24	26	.	.	PUNCT
eurjchem-289	25	1	unfortunately	unfortunately	ADV
eurjchem-289	25	2	,	,	PUNCT
eurjchem-289	25	3	none	none	NOUN
eurjchem-289	25	4	of	of	ADP
eurjchem-289	25	5	the	the	DET
eurjchem-289	25	6	tested	test	VERB
eurjchem-289	25	7	compounds	compound	NOUN
eurjchem-289	25	8	showed	show	VERB
eurjchem-289	25	9	any	any	DET
eurjchem-289	25	10	inhibitory	inhibitory	ADJ
eurjchem-289	25	11	activity	activity	NOUN
eurjchem-289	25	12	.	.	PUNCT
eurjchem-289	26	1	on	on	ADP
eurjchem-289	26	2	the	the	DET
eurjchem-289	26	3	other	other	ADJ
eurjchem-289	26	4	hand	hand	NOUN
eurjchem-289	26	5	,	,	PUNCT
eurjchem-289	26	6	some	some	DET
eurjchem-289	26	7	quinoxaline	quinoxaline	ADJ
eurjchem-289	26	8	derivatives	derivative	NOUN
eurjchem-289	26	9	were	be	AUX
eurjchem-289	26	10	found	find	VERB
eurjchem-289	26	11	to	to	PART
eurjchem-289	26	12	have	have	VERB
eurjchem-289	26	13	good	good	ADJ
eurjchem-289	26	14	antibacterial	antibacterial	ADJ
eurjchem-289	26	15	activity	activity	NOUN
eurjchem-289	26	16	against	against	ADP
eurjchem-289	26	17	staphylococcus	staphylococcus	NOUN
eurjchem-289	26	18	aureus	aureus	NOUN
eurjchem-289	26	19	and	and	CCONJ
eurjchem-289	26	20	bacillus	bacillus	NOUN
eurjchem-289	26	21	subtilis	subtili	NOUN
eurjchem-289	26	22	which	which	PRON
eurjchem-289	26	23	was	be	AUX
eurjchem-289	26	24	more	more	ADV
eurjchem-289	26	25	potent	potent	ADJ
eurjchem-289	26	26	than	than	ADP
eurjchem-289	26	27	tetracycline	tetracycline	NOUN
eurjchem-289	26	28	.	.	PUNCT
eurjchem-289	27	1	therefore	therefore	ADV
eurjchem-289	27	2	,	,	PUNCT
eurjchem-289	27	3	it	it	PRON
eurjchem-289	27	4	was	be	AUX
eurjchem-289	27	5	interesting	interesting	ADJ
eurjchem-289	27	6	to	to	PART
eurjchem-289	27	7	test	test	VERB
eurjchem-289	27	8	the	the	DET
eurjchem-289	27	9	antibacterial	antibacterial	ADJ
eurjchem-289	27	10	and	and	CCONJ
eurjchem-289	27	11	antifungal	antifungal	ADJ
eurjchem-289	27	12	activities	activity	NOUN
eurjchem-289	27	13	of	of	ADP
eurjchem-289	27	14	new	new	ADJ
eurjchem-289	27	15	quinoxalines	quinoxaline	NOUN
eurjchem-289	27	16	.	.	PUNCT
eurjchem-289	28	1	2	2	X
eurjchem-289	28	2	.	.	X
eurjchem-289	28	3	experimental	experimental	ADJ
eurjchem-289	28	4	2.1	2.1	NUM
eurjchem-289	28	5	.	.	PUNCT
eurjchem-289	29	1	chemistry	chemistry	NOUN
eurjchem-289	29	2	melting	melting	NOUN
eurjchem-289	29	3	points	point	NOUN
eurjchem-289	29	4	were	be	AUX
eurjchem-289	29	5	determined	determine	VERB
eurjchem-289	29	6	on	on	ADP
eurjchem-289	29	7	a	a	DET
eurjchem-289	29	8	griffin	griffin	NOUN
eurjchem-289	29	9	apparatus	apparatus	NOUN
eurjchem-289	29	10	and	and	CCONJ
eurjchem-289	29	11	were	be	AUX
eurjchem-289	29	12	uncorrected	uncorrecte	VERB
eurjchem-289	29	13	.	.	PUNCT
eurjchem-289	30	1	ir	ir	PROPN
eurjchem-289	30	2	spectra	spectra	PROPN
eurjchem-289	30	3	were	be	AUX
eurjchem-289	30	4	determined	determine	VERB
eurjchem-289	30	5	as	as	SCONJ
eurjchem-289	30	6	kbr	kbr	PROPN
eurjchem-289	30	7	discs	disc	NOUN
eurjchem-289	30	8	on	on	ADP
eurjchem-289	30	9	shimadzu	shimadzu	PROPN
eurjchem-289	30	10	ir	ir	PROPN
eurjchem-289	30	11	435	435	NUM
eurjchem-289	30	12	spectrophotometer	spectrophotometer	NOUN
eurjchem-289	30	13	and	and	CCONJ
eurjchem-289	30	14	values	value	NOUN
eurjchem-289	30	15	were	be	AUX
eurjchem-289	30	16	represented	represent	VERB
eurjchem-289	30	17	in	in	ADP
eurjchem-289	30	18	cm‐1	cm‐1	PROPN
eurjchem-289	30	19	.	.	PUNCT
eurjchem-289	31	1	1h	1h	NUM
eurjchem-289	31	2	nmr	nmr	NOUN
eurjchem-289	31	3	was	be	AUX
eurjchem-289	31	4	carried	carry	VERB
eurjchem-289	31	5	out	out	ADP
eurjchem-289	31	6	on	on	ADP
eurjchem-289	31	7	varian	varian	PROPN
eurjchem-289	31	8	gemini	gemini	PROPN
eurjchem-289	31	9	200	200	NUM
eurjchem-289	31	10	mhz	mhz	NOUN
eurjchem-289	31	11	and	and	CCONJ
eurjchem-289	31	12	300	300	NUM
eurjchem-289	31	13	mhz	mhz	NOUN
eurjchem-289	31	14	spectrophotometer	spectrophotometer	NOUN
eurjchem-289	31	15	,	,	PUNCT
eurjchem-289	31	16	microanalytical	microanalytical	ADJ
eurjchem-289	31	17	center	center	NOUN
eurjchem-289	31	18	,	,	PUNCT
eurjchem-289	31	19	cairo	cairo	PROPN
eurjchem-289	31	20	university	university	PROPN
eurjchem-289	31	21	,	,	PUNCT
eurjchem-289	31	22	egypt	egypt	PROPN
eurjchem-289	31	23	,	,	PUNCT
eurjchem-289	31	24	using	use	VERB
eurjchem-289	31	25	tms	tms	PROPN
eurjchem-289	31	26	as	as	SCONJ
eurjchem-289	31	27	an	an	DET
eurjchem-289	31	28	internal	internal	ADJ
eurjchem-289	31	29	standard	standard	ADJ
eurjchem-289	31	30	and	and	CCONJ
eurjchem-289	31	31	chemical	chemical	NOUN
eurjchem-289	31	32	shifts	shift	NOUN
eurjchem-289	31	33	were	be	AUX
eurjchem-289	31	34	recorded	record	VERB
eurjchem-289	31	35	in	in	ADP
eurjchem-289	31	36	ppm	ppm	NOUN
eurjchem-289	31	37	on	on	ADP
eurjchem-289	31	38	δ	δ	PROPN
eurjchem-289	31	39	scale	scale	NOUN
eurjchem-289	31	40	.	.	PUNCT
eurjchem-289	32	1	mass	mass	PROPN
eurjchem-289	32	2	spectra	spectra	PROPN
eurjchem-289	32	3	were	be	AUX
eurjchem-289	32	4	run	run	VERB
eurjchem-289	32	5	on	on	ADP
eurjchem-289	32	6	a	a	DET
eurjchem-289	32	7	hewlett	hewlett	PROPN
eurjchem-289	32	8	packard	packard	PROPN
eurjchem-289	32	9	5988	5988	NUM
eurjchem-289	32	10	spectrometer	spectrometer	NOUN
eurjchem-289	32	11	,	,	PUNCT
eurjchem-289	32	12	microanalytical	microanalytical	ADJ
eurjchem-289	32	13	center	center	NOUN
eurjchem-289	32	14	,	,	PUNCT
eurjchem-289	32	15	cairo	cairo	PROPN
eurjchem-289	32	16	university	university	NOUN
eurjchem-289	32	17	;	;	PUNCT
eurjchem-289	32	18	elemental	elemental	ADJ
eurjchem-289	32	19	analyses	analysis	NOUN
eurjchem-289	32	20	were	be	AUX
eurjchem-289	32	21	carried	carry	VERB
eurjchem-289	32	22	out	out	ADP
eurjchem-289	32	23	at	at	ADP
eurjchem-289	32	24	the	the	DET
eurjchem-289	32	25	microanalytical	microanalytical	ADJ
eurjchem-289	32	26	center	center	NOUN
eurjchem-289	32	27	,	,	PUNCT
eurjchem-289	32	28	cairo	cairo	PROPN
eurjchem-289	32	29	university	university	PROPN
eurjchem-289	32	30	.	.	PUNCT
eurjchem-289	33	1	progress	progress	NOUN
eurjchem-289	33	2	of	of	ADP
eurjchem-289	33	3	the	the	DET
eurjchem-289	33	4	reactions	reaction	NOUN
eurjchem-289	33	5	was	be	AUX
eurjchem-289	33	6	monitored	monitor	VERB
eurjchem-289	33	7	by	by	ADP
eurjchem-289	33	8	thin‐layer	thin‐layer	NOUN
eurjchem-289	33	9	chromatography	chromatography	NOUN
eurjchem-289	33	10	(	(	PUNCT
eurjchem-289	33	11	tlc	tlc	NOUN
eurjchem-289	33	12	)	)	PUNCT
eurjchem-289	33	13	using	use	VERB
eurjchem-289	33	14	tlc	tlc	NOUN
eurjchem-289	33	15	sheets	sheet	NOUN
eurjchem-289	33	16	pre‐coated	pre‐coate	VERB
eurjchem-289	33	17	with	with	ADP
eurjchem-289	33	18	uv	uv	NOUN
eurjchem-289	33	19	fluorescent	fluorescent	NOUN
eurjchem-289	33	20	silica	silica	NOUN
eurjchem-289	33	21	gel	gel	NOUN
eurjchem-289	33	22	merck	merck	PROPN
eurjchem-289	34	1	60	60	NUM
eurjchem-289	35	1	f254	f254	PROPN
eurjchem-289	36	1	that	that	PRON
eurjchem-289	36	2	were	be	AUX
eurjchem-289	36	3	visualized	visualize	VERB
eurjchem-289	36	4	using	use	VERB
eurjchem-289	36	5	uv	uv	NOUN
eurjchem-289	36	6	lamp	lamp	NOUN
eurjchem-289	36	7	.	.	PUNCT
eurjchem-289	37	1	2.2	2.2	NUM
eurjchem-289	37	2	.	.	PUNCT
eurjchem-289	38	1	synthesis	synthesis	NOUN
eurjchem-289	38	2	2.2.1	2.2.1	NUM
eurjchem-289	38	3	.	.	PUNCT
eurjchem-289	39	1	ethyl	ethyl	PROPN
eurjchem-289	39	2	acetylpyruvate	acetylpyruvate	PROPN
eurjchem-289	39	3	sodium	sodium	NOUN
eurjchem-289	39	4	salt	salt	NOUN
eurjchem-289	39	5	1,3‐acetonylquino‐	1,3‐acetonylquino‐	PROPN
eurjchem-289	39	6	xalin‐2(1h)‐one	xalin‐2(1h)‐one	PROPN
eurjchem-289	39	7	2,3‐(2‐oxo‐4‐phenylbut‐3‐en‐1‐yl	2,3‐(2‐oxo‐4‐phenylbut‐3‐en‐1‐yl	NUM
eurjchem-289	39	8	)	)	PUNCT
eurjchem-289	39	9	quinoxalin‐2(1h)‐ones	quinoxalin‐2(1h)‐one	NOUN
eurjchem-289	39	10	(	(	PUNCT
eurjchem-289	39	11	3a	3a	NUM
eurjchem-289	39	12	)	)	PUNCT
eurjchem-289	39	13	and	and	CCONJ
eurjchem-289	39	14	3‐(2‐oxo‐4‐(4‐chloro	3‐(2‐oxo‐4‐(4‐chloro	NUM
eurjchem-289	39	15	phenyl)‐but‐3‐en‐1‐yl)quinoxalin‐2(1h)‐ones	phenyl)‐but‐3‐en‐1‐yl)quinoxalin‐2(1h)‐one	NOUN
eurjchem-289	39	16	(	(	PUNCT
eurjchem-289	39	17	3b	3b	NUM
eurjchem-289	39	18	)	)	PUNCT
eurjchem-289	39	19	ethyl	ethyl	PROPN
eurjchem-289	39	20	acetylpyruvate	acetylpyruvate	PROPN
eurjchem-289	39	21	sodium	sodium	NOUN
eurjchem-289	39	22	salt	salt	NOUN
eurjchem-289	39	23	1,3‐acetonylquinoxalin‐	1,3‐acetonylquinoxalin‐	NUM
eurjchem-289	39	24	2(1h)‐one	2(1h)‐one	NUM
eurjchem-289	39	25	2,3‐(2‐oxo‐4‐phenylbut‐3‐en‐1‐yl)quinoxalin‐2(1h)‐	2,3‐(2‐oxo‐4‐phenylbut‐3‐en‐1‐yl)quinoxalin‐2(1h)‐	NOUN
eurjchem-289	39	26	366	366	NUM
eurjchem-289	39	27	shabaan	shabaan	X
eurjchem-289	39	28	et	et	PROPN
eurjchem-289	39	29	al	al	PROPN
eurjchem-289	39	30	.	.	PUNCT
eurjchem-289	39	31	/	/	SYM
eurjchem-289	39	32	european	european	PROPN
eurjchem-289	39	33	journal	journal	PROPN
eurjchem-289	39	34	of	of	ADP
eurjchem-289	39	35	chemistry	chemistry	NOUN
eurjchem-289	39	36	2	2	NUM
eurjchem-289	39	37	(	(	PUNCT
eurjchem-289	39	38	3	3	NUM
eurjchem-289	39	39	)	)	PUNCT
eurjchem-289	39	40	(	(	PUNCT
eurjchem-289	39	41	2011	2011	NUM
eurjchem-289	39	42	)	)	PUNCT
eurjchem-289	40	1	365‐371	365‐371	NUM
eurjchem-289	40	2	n	n	NUM
eurjchem-289	40	3	h	h	NOUN
eurjchem-289	40	4	n	n	ADV
eurjchem-289	40	5	o	o	NOUN
eurjchem-289	40	6	o	o	NOUN
eurjchem-289	40	7	n	n	CCONJ
eurjchem-289	40	8	h	h	NOUN
eurjchem-289	40	9	n	n	ADP
eurjchem-289	40	10	o	o	NOUN
eurjchem-289	40	11	o	o	X
eurjchem-289	40	12	ar	ar	PROPN
eurjchem-289	40	13	n	n	PROPN
eurjchem-289	40	14	h	h	NOUN
eurjchem-289	40	15	n	n	ADV
eurjchem-289	40	16	o	o	NOUN
eurjchem-289	40	17	o	o	NOUN
eurjchem-289	40	18	n	n	ADP
eurjchem-289	40	19	archo	archo	NOUN
eurjchem-289	41	1	n	n	PRON
eurjchem-289	41	2	h	h	NOUN
eurjchem-289	41	3	n	n	ADV
eurjchem-289	41	4	o	o	NOUN
eurjchem-289	41	5	o	o	NOUN
eurjchem-289	41	6	paraformaldehyde	paraformaldehyde	NOUN
eurjchem-289	41	7	naoh	naoh	NOUN
eurjchem-289	41	8	arn	arn	PROPN
eurjchem-289	41	9	h	h	PROPN
eurjchem-289	42	1	n	n	PROPN
eurjchem-289	42	2	hn	hn	NOUN
eurjchem-289	42	3	o	o	X
eurjchem-289	42	4	nh	nh	PROPN
eurjchem-289	42	5	cn	cn	PROPN
eurjchem-289	42	6	phcho	phcho	PROPN
eurjchem-289	42	7	/	/	SYM
eurjchem-289	42	8	acetic	acetic	ADJ
eurjchem-289	42	9	acid	acid	NOUN
eurjchem-289	42	10	/	/	SYM
eurjchem-289	42	11	reflux	reflux	NOUN
eurjchem-289	42	12	h	h	NOUN
eurjchem-289	42	13	n	n	CCONJ
eurjchem-289	42	14	n	n	NOUN
eurjchem-289	42	15	o	o	NOUN
eurjchem-289	42	16	o	o	X
eurjchem-289	42	17	8	8	NUM
eurjchem-289	42	18	ethyl	ethyl	PROPN
eurjchem-289	42	19	cyanoacetate	cyanoacetate	NOUN
eurjchem-289	42	20	ammonium	ammonium	NOUN
eurjchem-289	42	21	acetate	acetate	PROPN
eurjchem-289	42	22	archo	archo	PROPN
eurjchem-289	42	23	malononitrile	malononitrile	PROPN
eurjchem-289	42	24	ammonium	ammonium	NOUN
eurjchem-289	42	25	acetate	acetate	PROPN
eurjchem-289	42	26	archoacetic	archoacetic	ADJ
eurjchem-289	42	27	acid	acid	NOUN
eurjchem-289	42	28	or	or	CCONJ
eurjchem-289	42	29	phcho	phcho	NOUN
eurjchem-289	42	30	/	/	SYM
eurjchem-289	42	31	fusion	fusion	NOUN
eurjchem-289	42	32	br2	br2	PROPN
eurjchem-289	42	33	/	/	SYM
eurjchem-289	42	34	acetic	acetic	ADJ
eurjchem-289	42	35	acid	acid	NOUN
eurjchem-289	42	36	/	/	SYM
eurjchem-289	42	37	sodium	sodium	NOUN
eurjchem-289	42	38	acetate	acetate	NOUN
eurjchem-289	42	39	or	or	CCONJ
eurjchem-289	42	40	reflux	reflux	NOUN
eurjchem-289	42	41	in	in	ADP
eurjchem-289	42	42	ethylene	ethylene	NOUN
eurjchem-289	42	43	glycol	glycol	NOUN
eurjchem-289	42	44	n	n	CCONJ
eurjchem-289	42	45	h	h	NOUN
eurjchem-289	42	46	n	n	ADV
eurjchem-289	43	1	hn	hn	NOUN
eurjchem-289	44	1	o	o	X
eurjchem-289	44	2	o	o	X
eurjchem-289	44	3	cn	cn	PROPN
eurjchem-289	44	4	ar	ar	PROPN
eurjchem-289	44	5	n	n	PROPN
eurjchem-289	44	6	n	n	PROPN
eurjchem-289	44	7	o	o	PROPN
eurjchem-289	44	8	ar	ar	PROPN
eurjchem-289	44	9	n	n	PROPN
eurjchem-289	44	10	h	h	PROPN
eurjchem-289	44	11	n	n	CCONJ
eurjchem-289	44	12	nhn	nhn	PROPN
eurjchem-289	44	13	ar	ar	PROPN
eurjchem-289	44	14	h2so4	h2so4	PROPN
eurjchem-289	44	15	nh2nh2	nh2nh2	NOUN
eurjchem-289	44	16	ethanol	ethanol	VERB
eurjchem-289	44	17	o	o	NOUN
eurjchem-289	44	18	nh2	nh2	PROPN
eurjchem-289	44	19	nh2	nh2	PROPN
eurjchem-289	45	1	o	o	NOUN
eurjchem-289	45	2	o	o	X
eurjchem-289	45	3	o	o	NOUN
eurjchem-289	45	4	1	1	NUM
eurjchem-289	45	5	ethanol	ethanol	NOUN
eurjchem-289	45	6	ethanol	ethanol	NOUN
eurjchem-289	45	7	acetic	acetic	ADJ
eurjchem-289	45	8	anhydride	anhydride	NOUN
eurjchem-289	45	9	+	+	CCONJ
eurjchem-289	45	10	2	2	NUM
eurjchem-289	45	11	3	3	NUM
eurjchem-289	45	12	4	4	NUM
eurjchem-289	45	13	5a	5a	NUM
eurjchem-289	45	14	,	,	PUNCT
eurjchem-289	45	15	b	b	NOUN
eurjchem-289	45	16	6a	6a	NOUN
eurjchem-289	45	17	-	-	PUNCT
eurjchem-289	45	18	c	c	NOUN
eurjchem-289	45	19	7	7	NUM
eurjchem-289	45	20	10a	10a	NOUN
eurjchem-289	45	21	,	,	PUNCT
eurjchem-289	45	22	b	b	NOUN
eurjchem-289	45	23	9a	9a	NOUN
eurjchem-289	45	24	,	,	PUNCT
eurjchem-289	45	25	b	b	PROPN
eurjchem-289	45	26	ar	ar	NOUN
eurjchem-289	45	27	=	=	PROPN
eurjchem-289	45	28	c6h5	c6h5	PROPN
eurjchem-289	45	29	p	p	PROPN
eurjchem-289	45	30	-	-	PROPN
eurjchem-289	45	31	clc6h4	clc6h4	NOUN
eurjchem-289	45	32	m	m	PROPN
eurjchem-289	45	33	-	-	PROPN
eurjchem-289	45	34	no2c6h4	no2c6h4	ADJ
eurjchem-289	45	35	p	p	ADJ
eurjchem-289	45	36	-	-	PUNCT
eurjchem-289	45	37	fc6h4	fc6h4	ADJ
eurjchem-289	45	38	acetic	acetic	ADJ
eurjchem-289	45	39	acid	acid	NOUN
eurjchem-289	45	40	scheme	scheme	NOUN
eurjchem-289	45	41	1	1	NUM
eurjchem-289	45	42	ones	one	NOUN
eurjchem-289	45	43	(	(	PUNCT
eurjchem-289	45	44	3a	3a	NUM
eurjchem-289	45	45	)	)	PUNCT
eurjchem-289	45	46	,	,	PUNCT
eurjchem-289	45	47	3‐(2‐oxo‐4‐(4‐chlorophenyl)‐but‐3‐en‐1‐yl	3‐(2‐oxo‐4‐(4‐chlorophenyl)‐but‐3‐en‐1‐yl	NUM
eurjchem-289	45	48	)	)	PUNCT
eurjchem-289	45	49	quino‐	quino‐	VERB
eurjchem-289	45	50	xalin‐2(1h)‐ones	xalin‐2(1h)‐one	NOUN
eurjchem-289	45	51	(	(	PUNCT
eurjchem-289	45	52	3b	3b	NUM
eurjchem-289	45	53	)	)	PUNCT
eurjchem-289	45	54	were	be	AUX
eurjchem-289	45	55	prepared	prepare	VERB
eurjchem-289	45	56	as	as	SCONJ
eurjchem-289	45	57	reported	report	VERB
eurjchem-289	45	58	[	[	X
eurjchem-289	45	59	23‐25	23‐25	X
eurjchem-289	45	60	]	]	X
eurjchem-289	45	61	(	(	PUNCT
eurjchem-289	45	62	scheme	scheme	NOUN
eurjchem-289	45	63	1	1	NUM
eurjchem-289	45	64	)	)	PUNCT
eurjchem-289	45	65	.	.	PUNCT
eurjchem-289	46	1	2.2.2	2.2.2	NUM
eurjchem-289	46	2	.	.	X
eurjchem-289	46	3	3‐(2‐oxo‐4‐(3‐nitrophenyl)‐but‐3‐en‐1‐yl)quinoxalin‐	3‐(2‐oxo‐4‐(3‐nitrophenyl)‐but‐3‐en‐1‐yl)quinoxalin‐	NUM
eurjchem-289	46	4	2(1h)‐ones	2(1h)‐ones	NUM
eurjchem-289	46	5	(	(	PUNCT
eurjchem-289	46	6	3c	3c	NUM
eurjchem-289	46	7	)	)	PUNCT
eurjchem-289	46	8	and	and	CCONJ
eurjchem-289	46	9	3‐(2‐oxo‐4‐(4‐flourophenyl)‐but‐3‐en‐1‐	3‐(2‐oxo‐4‐(4‐flourophenyl)‐but‐3‐en‐1‐	NUM
eurjchem-289	46	10	yl)quinoxalin‐2(1h)‐ones	yl)quinoxalin‐2(1h)‐one	NOUN
eurjchem-289	46	11	(	(	PUNCT
eurjchem-289	46	12	3d	3d	NOUN
eurjchem-289	46	13	)	)	PUNCT
eurjchem-289	46	14	to	to	ADP
eurjchem-289	46	15	a	a	DET
eurjchem-289	46	16	suspension	suspension	NOUN
eurjchem-289	46	17	of	of	ADP
eurjchem-289	46	18	3‐acetonylquinoxalin‐2(1h)‐one(2	3‐acetonylquinoxalin‐2(1h)‐one(2	NOUN
eurjchem-289	46	19	)	)	PUNCT
eurjchem-289	46	20	(	(	PUNCT
eurjchem-289	46	21	0.5	0.5	NUM
eurjchem-289	46	22	g	g	NOUN
eurjchem-289	46	23	,	,	PUNCT
eurjchem-289	46	24	0.0025	0.0025	NUM
eurjchem-289	46	25	mol	mol	NOUN
eurjchem-289	46	26	)	)	PUNCT
eurjchem-289	46	27	in	in	ADP
eurjchem-289	46	28	water	water	NOUN
eurjchem-289	46	29	(	(	PUNCT
eurjchem-289	46	30	10	10	NUM
eurjchem-289	46	31	ml	ml	NOUN
eurjchem-289	46	32	)	)	PUNCT
eurjchem-289	46	33	and	and	CCONJ
eurjchem-289	46	34	10	10	NUM
eurjchem-289	46	35	%	%	NOUN
eurjchem-289	46	36	sodium	sodium	NOUN
eurjchem-289	46	37	hydroxide	hydroxide	NOUN
eurjchem-289	46	38	(	(	PUNCT
eurjchem-289	46	39	2	2	NUM
eurjchem-289	46	40	ml	ml	NOUN
eurjchem-289	46	41	)	)	PUNCT
eurjchem-289	46	42	,	,	PUNCT
eurjchem-289	46	43	the	the	DET
eurjchem-289	46	44	appropriate	appropriate	ADJ
eurjchem-289	46	45	aldehyde	aldehyde	NOUN
eurjchem-289	46	46	(	(	PUNCT
eurjchem-289	46	47	0.0025	0.0025	NUM
eurjchem-289	46	48	mol	mol	NOUN
eurjchem-289	46	49	)	)	PUNCT
eurjchem-289	46	50	was	be	AUX
eurjchem-289	46	51	sequentially	sequentially	ADV
eurjchem-289	46	52	added	add	VERB
eurjchem-289	46	53	with	with	ADP
eurjchem-289	46	54	continuous	continuous	ADJ
eurjchem-289	46	55	stirring	stirring	NOUN
eurjchem-289	46	56	.	.	PUNCT
eurjchem-289	47	1	the	the	DET
eurjchem-289	47	2	formed	form	VERB
eurjchem-289	47	3	solid	solid	ADJ
eurjchem-289	47	4	product	product	NOUN
eurjchem-289	47	5	was	be	AUX
eurjchem-289	47	6	filtered	filter	VERB
eurjchem-289	47	7	,	,	PUNCT
eurjchem-289	47	8	dried	dry	VERB
eurjchem-289	47	9	and	and	CCONJ
eurjchem-289	47	10	crystallized	crystallize	VERB
eurjchem-289	47	11	from	from	ADP
eurjchem-289	47	12	acetone	acetone	NOUN
eurjchem-289	47	13	(	(	PUNCT
eurjchem-289	47	14	scheme	scheme	NOUN
eurjchem-289	47	15	1	1	NUM
eurjchem-289	47	16	)	)	PUNCT
eurjchem-289	47	17	.	.	PUNCT
eurjchem-289	48	1	3‐(2‐oxo‐4‐(3‐nitrophenyl)‐but‐3‐en‐1‐yl)quinoxalin‐2(1h)‐	3‐(2‐oxo‐4‐(3‐nitrophenyl)‐but‐3‐en‐1‐yl)quinoxalin‐2(1h)‐	NUM
eurjchem-289	48	2	ones	one	NOUN
eurjchem-289	48	3	(	(	PUNCT
eurjchem-289	48	4	3c	3c	NUM
eurjchem-289	48	5	)	)	PUNCT
eurjchem-289	48	6	:	:	PUNCT
eurjchem-289	48	7	yield	yield	NOUN
eurjchem-289	48	8	:	:	PUNCT
eurjchem-289	48	9	65	65	NUM
eurjchem-289	48	10	%	%	NOUN
eurjchem-289	48	11	.	.	PUNCT
eurjchem-289	49	1	m.p	m.p	PROPN
eurjchem-289	49	2	.	.	PROPN
eurjchem-289	49	3	:	:	PUNCT
eurjchem-289	50	1	210‐212	210‐212	NUM
eurjchem-289	50	2	οc	οc	ADP
eurjchem-289	50	3	.	.	PROPN
eurjchem-289	50	4	ir	ir	PROPN
eurjchem-289	50	5	(	(	PUNCT
eurjchem-289	50	6	kbr	kbr	PROPN
eurjchem-289	50	7	,	,	PUNCT
eurjchem-289	50	8	cm‐1	cm‐1	PROPN
eurjchem-289	50	9	):	):	PUNCT
eurjchem-289	50	10	3450	3450	NUM
eurjchem-289	50	11	,	,	PUNCT
eurjchem-289	50	12	3400	3400	NUM
eurjchem-289	50	13	(	(	PUNCT
eurjchem-289	50	14	nh	nh	NOUN
eurjchem-289	50	15	)	)	PUNCT
eurjchem-289	50	16	,	,	PUNCT
eurjchem-289	50	17	1685	1685	NUM
eurjchem-289	50	18	,	,	PUNCT
eurjchem-289	50	19	1680	1680	NUM
eurjchem-289	50	20	(	(	PUNCT
eurjchem-289	50	21	c	c	NOUN
eurjchem-289	50	22	=	=	NOUN
eurjchem-289	50	23	o	o	NOUN
eurjchem-289	50	24	)	)	PUNCT
eurjchem-289	50	25	,	,	PUNCT
eurjchem-289	50	26	1620(c	1620(c	NOUN
eurjchem-289	50	27	=	=	SYM
eurjchem-289	50	28	n	n	NUM
eurjchem-289	50	29	)	)	PUNCT
eurjchem-289	50	30	.	.	PUNCT
eurjchem-289	51	1	1h	1h	NUM
eurjchem-289	51	2	nmr	nmr	NOUN
eurjchem-289	51	3	(	(	PUNCT
eurjchem-289	51	4	dmso‐d6	dmso‐d6	PROPN
eurjchem-289	51	5	,	,	PUNCT
eurjchem-289	51	6	δ	δ	PROPN
eurjchem-289	51	7	,	,	PUNCT
eurjchem-289	51	8	ppm	ppm	NUM
eurjchem-289	51	9	):	):	PUNCT
eurjchem-289	51	10	6.35	6.35	NUM
eurjchem-289	51	11	(	(	PUNCT
eurjchem-289	51	12	s	s	PROPN
eurjchem-289	51	13	,	,	PUNCT
eurjchem-289	51	14	1h	1h	NUM
eurjchem-289	51	15	,	,	PUNCT
eurjchem-289	51	16	vinylic	vinylic	ADJ
eurjchem-289	51	17	ch	ch	NOUN
eurjchem-289	51	18	)	)	PUNCT
eurjchem-289	51	19	,	,	PUNCT
eurjchem-289	51	20	7.10‐7.78	7.10‐7.78	NUM
eurjchem-289	51	21	(	(	PUNCT
eurjchem-289	51	22	m	m	PROPN
eurjchem-289	51	23	,	,	PUNCT
eurjchem-289	51	24	10h	10h	NUM
eurjchem-289	51	25	)	)	PUNCT
eurjchem-289	51	26	,	,	PUNCT
eurjchem-289	51	27	13.88‐	13.88‐	PROPN
eurjchem-289	51	28	14.00	14.00	NUM
eurjchem-289	51	29	(	(	PUNCT
eurjchem-289	51	30	br	br	PROPN
eurjchem-289	51	31	,	,	PUNCT
eurjchem-289	51	32	2h	2h	NUM
eurjchem-289	51	33	,	,	PUNCT
eurjchem-289	51	34	nh	nh	PROPN
eurjchem-289	51	35	,	,	PUNCT
eurjchem-289	51	36	oh	oh	INTJ
eurjchem-289	51	37	,	,	PUNCT
eurjchem-289	51	38	exchanged	exchange	VERB
eurjchem-289	51	39	with	with	ADP
eurjchem-289	51	40	d2o	d2o	NOUN
eurjchem-289	51	41	)	)	PUNCT
eurjchem-289	51	42	.	.	PUNCT
eurjchem-289	52	1	ms	ms	NOUN
eurjchem-289	52	2	(	(	PUNCT
eurjchem-289	52	3	m	m	PROPN
eurjchem-289	52	4	/	/	SYM
eurjchem-289	52	5	z	z	NOUN
eurjchem-289	52	6	(	(	PUNCT
eurjchem-289	52	7	%	%	NOUN
eurjchem-289	52	8	)	)	PUNCT
eurjchem-289	52	9	):	):	PUNCT
eurjchem-289	52	10	213	213	NUM
eurjchem-289	52	11	(	(	PUNCT
eurjchem-289	52	12	100	100	NUM
eurjchem-289	52	13	%	%	NOUN
eurjchem-289	52	14	)	)	PUNCT
eurjchem-289	52	15	,	,	PUNCT
eurjchem-289	52	16	335	335	NUM
eurjchem-289	52	17	(	(	PUNCT
eurjchem-289	52	18	m+	m+	NUM
eurjchem-289	52	19	.	.	PROPN
eurjchem-289	52	20	,	,	PUNCT
eurjchem-289	52	21	26.96	26.96	NUM
eurjchem-289	52	22	%	%	NOUN
eurjchem-289	52	23	)	)	PUNCT
eurjchem-289	52	24	,	,	PUNCT
eurjchem-289	52	25	336(m+1	336(m+1	NUM
eurjchem-289	52	26	┐	┐	PROPN
eurjchem-289	52	27	+	+	PROPN
eurjchem-289	52	28	.	.	PROPN
eurjchem-289	52	29	,	,	PUNCT
eurjchem-289	52	30	5.83	5.83	NUM
eurjchem-289	52	31	%	%	NOUN
eurjchem-289	52	32	)	)	PUNCT
eurjchem-289	52	33	.	.	PUNCT
eurjchem-289	53	1	anal	anal	PROPN
eurjchem-289	53	2	.	.	PUNCT
eurjchem-289	53	3	calcd.of	calcd.of	PROPN
eurjchem-289	53	4	c18h13n3o4	c18h13n3o4	PROPN
eurjchem-289	53	5	(	(	PUNCT
eurjchem-289	53	6	335	335	NUM
eurjchem-289	53	7	):	):	PUNCT
eurjchem-289	53	8	c	c	X
eurjchem-289	53	9	,	,	PUNCT
eurjchem-289	53	10	64.48	64.48	NUM
eurjchem-289	53	11	;	;	PUNCT
eurjchem-289	53	12	h	h	NOUN
eurjchem-289	53	13	,	,	PUNCT
eurjchem-289	53	14	3.88	3.88	NUM
eurjchem-289	53	15	;	;	PUNCT
eurjchem-289	53	16	n	n	CCONJ
eurjchem-289	53	17	,	,	PUNCT
eurjchem-289	53	18	12.54	12.54	NUM
eurjchem-289	53	19	.	.	PUNCT
eurjchem-289	53	20	found	find	VERB
eurjchem-289	53	21	:	:	PUNCT
eurjchem-289	54	1	c	c	X
eurjchem-289	54	2	,	,	PUNCT
eurjchem-289	54	3	64.71	64.71	NUM
eurjchem-289	54	4	;	;	PUNCT
eurjchem-289	54	5	h	h	X
eurjchem-289	54	6	,	,	PUNCT
eurjchem-289	54	7	3.97	3.97	NUM
eurjchem-289	54	8	;	;	PUNCT
eurjchem-289	54	9	n	n	CCONJ
eurjchem-289	54	10	,	,	PUNCT
eurjchem-289	54	11	12.68	12.68	NUM
eurjchem-289	54	12	%	%	NOUN
eurjchem-289	54	13	.	.	PUNCT
eurjchem-289	55	1	3‐(2‐oxo‐4‐(4‐flourophenyl)‐but‐3‐en‐1‐yl)quinoxalin‐2(1h)‐	3‐(2‐oxo‐4‐(4‐flourophenyl)‐but‐3‐en‐1‐yl)quinoxalin‐2(1h)‐	NUM
eurjchem-289	55	2	ones	one	NOUN
eurjchem-289	55	3	(	(	PUNCT
eurjchem-289	55	4	3d	3d	NOUN
eurjchem-289	55	5	)	)	PUNCT
eurjchem-289	55	6	:	:	PUNCT
eurjchem-289	55	7	yield	yield	NOUN
eurjchem-289	55	8	:	:	PUNCT
eurjchem-289	55	9	72	72	NUM
eurjchem-289	55	10	%	%	NOUN
eurjchem-289	55	11	.	.	PUNCT
eurjchem-289	56	1	m.p	m.p	PROPN
eurjchem-289	56	2	.	.	PROPN
eurjchem-289	56	3	:	:	PUNCT
eurjchem-289	57	1	213‐214	213‐214	NUM
eurjchem-289	57	2	οc	οc	NOUN
eurjchem-289	57	3	.	.	PROPN
eurjchem-289	57	4	ir	ir	PROPN
eurjchem-289	57	5	(	(	PUNCT
eurjchem-289	57	6	kbr	kbr	PROPN
eurjchem-289	57	7	,	,	PUNCT
eurjchem-289	57	8	cm‐1	cm‐1	PROPN
eurjchem-289	57	9	):	):	PUNCT
eurjchem-289	57	10	3400	3400	NUM
eurjchem-289	57	11	,	,	PUNCT
eurjchem-289	57	12	3350	3350	NUM
eurjchem-289	57	13	(	(	PUNCT
eurjchem-289	57	14	nh	nh	NOUN
eurjchem-289	57	15	)	)	PUNCT
eurjchem-289	57	16	,	,	PUNCT
eurjchem-289	57	17	1690	1690	NUM
eurjchem-289	57	18	,	,	PUNCT
eurjchem-289	57	19	1680	1680	NUM
eurjchem-289	57	20	(	(	PUNCT
eurjchem-289	57	21	c	c	NOUN
eurjchem-289	57	22	=	=	NOUN
eurjchem-289	57	23	o	o	NOUN
eurjchem-289	57	24	)	)	PUNCT
eurjchem-289	57	25	,	,	PUNCT
eurjchem-289	57	26	1630(c	1630(c	NOUN
eurjchem-289	57	27	=	=	SYM
eurjchem-289	57	28	n	n	CCONJ
eurjchem-289	57	29	)	)	PUNCT
eurjchem-289	57	30	.	.	PUNCT
eurjchem-289	58	1	1h	1h	NUM
eurjchem-289	58	2	nmr	nmr	NOUN
eurjchem-289	58	3	(	(	PUNCT
eurjchem-289	58	4	dmso‐d6	dmso‐d6	PROPN
eurjchem-289	58	5	,	,	PUNCT
eurjchem-289	58	6	δ	δ	PROPN
eurjchem-289	58	7	,	,	PUNCT
eurjchem-289	58	8	ppm	ppm	NUM
eurjchem-289	58	9	):	):	PUNCT
eurjchem-289	58	10	6.33	6.33	NUM
eurjchem-289	58	11	(	(	PUNCT
eurjchem-289	58	12	s	s	PROPN
eurjchem-289	58	13	,	,	PUNCT
eurjchem-289	58	14	1h	1h	NUM
eurjchem-289	58	15	,	,	PUNCT
eurjchem-289	58	16	vinylic	vinylic	ADJ
eurjchem-289	58	17	ch	ch	NOUN
eurjchem-289	58	18	)	)	PUNCT
eurjchem-289	58	19	,	,	PUNCT
eurjchem-289	58	20	7.05‐7.83	7.05‐7.83	NUM
eurjchem-289	58	21	(	(	PUNCT
eurjchem-289	58	22	m	m	PROPN
eurjchem-289	58	23	,	,	PUNCT
eurjchem-289	58	24	10h	10h	NUM
eurjchem-289	58	25	)	)	PUNCT
eurjchem-289	58	26	,	,	PUNCT
eurjchem-289	58	27	12.01	12.01	NUM
eurjchem-289	58	28	,	,	PUNCT
eurjchem-289	58	29	13.82	13.82	NUM
eurjchem-289	58	30	(	(	PUNCT
eurjchem-289	58	31	2s	2s	NUM
eurjchem-289	58	32	,	,	PUNCT
eurjchem-289	58	33	2h	2h	NUM
eurjchem-289	58	34	,	,	PUNCT
eurjchem-289	58	35	nh	nh	PROPN
eurjchem-289	58	36	,	,	PUNCT
eurjchem-289	58	37	oh	oh	INTJ
eurjchem-289	58	38	,	,	PUNCT
eurjchem-289	58	39	exchanged	exchange	VERB
eurjchem-289	58	40	with	with	ADP
eurjchem-289	58	41	d2o	d2o	NOUN
eurjchem-289	58	42	)	)	PUNCT
eurjchem-289	58	43	.	.	PUNCT
eurjchem-289	59	1	anal	anal	PROPN
eurjchem-289	59	2	.	.	PUNCT
eurjchem-289	59	3	calcd	calcd	NOUN
eurjchem-289	59	4	.	.	PUNCT
eurjchem-289	60	1	for	for	SCONJ
eurjchem-289	60	2	c18h13fn2o2	c18h13fn2o2	PROPN
eurjchem-289	60	3	(	(	PUNCT
eurjchem-289	60	4	308	308	NUM
eurjchem-289	60	5	):	):	PUNCT
eurjchem-289	60	6	c	c	NOUN
eurjchem-289	60	7	,	,	PUNCT
eurjchem-289	60	8	70.12	70.12	NUM
eurjchem-289	60	9	;	;	PUNCT
eurjchem-289	60	10	h	h	X
eurjchem-289	60	11	,	,	PUNCT
eurjchem-289	60	12	4.23	4.23	NUM
eurjchem-289	60	13	;	;	PUNCT
eurjchem-289	60	14	n	n	CCONJ
eurjchem-289	60	15	,	,	PUNCT
eurjchem-289	60	16	9.09	9.09	NUM
eurjchem-289	60	17	.	.	PUNCT
eurjchem-289	60	18	found	find	VERB
eurjchem-289	60	19	:	:	PUNCT
eurjchem-289	61	1	c	c	X
eurjchem-289	61	2	,	,	PUNCT
eurjchem-289	61	3	70.33	70.33	NUM
eurjchem-289	61	4	;	;	PUNCT
eurjchem-289	61	5	h	h	NOUN
eurjchem-289	61	6	,	,	PUNCT
eurjchem-289	61	7	4.22	4.22	NUM
eurjchem-289	61	8	;	;	PUNCT
eurjchem-289	61	9	n	n	CCONJ
eurjchem-289	61	10	,	,	PUNCT
eurjchem-289	61	11	8.79	8.79	NUM
eurjchem-289	61	12	%	%	NOUN
eurjchem-289	61	13	.	.	PUNCT
eurjchem-289	62	1	2.2.3	2.2.3	X
eurjchem-289	62	2	.	.	X
eurjchem-289	63	1	10‐phenyl‐5h‐pyrido[1,2‐a]quinoxaline‐6,8‐dione	10‐phenyl‐5h‐pyrido[1,2‐a]quinoxaline‐6,8‐dione	NUM
eurjchem-289	63	2	(	(	PUNCT
eurjchem-289	63	3	4	4	NUM
eurjchem-289	63	4	)	)	PUNCT
eurjchem-289	63	5	method	method	NOUN
eurjchem-289	63	6	a	a	DET
eurjchem-289	63	7	:	:	PUNCT
eurjchem-289	63	8	benzaldehyde	benzaldehyde	NOUN
eurjchem-289	63	9	(	(	PUNCT
eurjchem-289	63	10	0.53	0.53	NUM
eurjchem-289	63	11	g	g	NOUN
eurjchem-289	63	12	,	,	PUNCT
eurjchem-289	63	13	0.005	0.005	NUM
eurjchem-289	63	14	mol	mol	NOUN
eurjchem-289	63	15	)	)	PUNCT
eurjchem-289	63	16	was	be	AUX
eurjchem-289	63	17	added	add	VERB
eurjchem-289	63	18	to	to	ADP
eurjchem-289	63	19	a	a	DET
eurjchem-289	63	20	solution	solution	NOUN
eurjchem-289	63	21	of	of	ADP
eurjchem-289	63	22	2	2	NUM
eurjchem-289	63	23	(	(	PUNCT
eurjchem-289	63	24	1.01	1.01	NUM
eurjchem-289	63	25	g	g	NOUN
eurjchem-289	63	26	,	,	PUNCT
eurjchem-289	63	27	0.005	0.005	NUM
eurjchem-289	63	28	mol	mol	NOUN
eurjchem-289	63	29	)	)	PUNCT
eurjchem-289	63	30	in	in	ADP
eurjchem-289	63	31	acetic	acetic	ADJ
eurjchem-289	63	32	acid	acid	NOUN
eurjchem-289	63	33	(	(	PUNCT
eurjchem-289	63	34	25	25	NUM
eurjchem-289	63	35	ml	ml	NOUN
eurjchem-289	63	36	)	)	PUNCT
eurjchem-289	63	37	.	.	PUNCT
eurjchem-289	64	1	the	the	DET
eurjchem-289	64	2	mixture	mixture	NOUN
eurjchem-289	64	3	was	be	AUX
eurjchem-289	64	4	heated	heat	VERB
eurjchem-289	64	5	under	under	ADP
eurjchem-289	64	6	reflux	reflux	NOUN
eurjchem-289	64	7	for	for	SCONJ
eurjchem-289	64	8	5	5	NUM
eurjchem-289	64	9	h.	h.	NOUN
eurjchem-289	64	10	the	the	DET
eurjchem-289	64	11	product	product	NOUN
eurjchem-289	64	12	formed	form	VERB
eurjchem-289	64	13	was	be	AUX
eurjchem-289	64	14	filtered	filter	VERB
eurjchem-289	64	15	and	and	CCONJ
eurjchem-289	64	16	crystallized	crystallize	VERB
eurjchem-289	64	17	from	from	ADP
eurjchem-289	64	18	ethanol	ethanol	NOUN
eurjchem-289	64	19	(	(	PUNCT
eurjchem-289	64	20	scheme	scheme	NOUN
eurjchem-289	64	21	1	1	NUM
eurjchem-289	64	22	)	)	PUNCT
eurjchem-289	64	23	.	.	PUNCT
eurjchem-289	65	1	yield	yield	NOUN
eurjchem-289	65	2	:	:	PUNCT
eurjchem-289	65	3	75	75	NUM
eurjchem-289	65	4	%	%	NOUN
eurjchem-289	65	5	.	.	PUNCT
eurjchem-289	66	1	m.p	m.p	PROPN
eurjchem-289	66	2	.	.	PROPN
eurjchem-289	66	3	:	:	PUNCT
eurjchem-289	67	1	>	>	PUNCT
eurjchem-289	67	2	300	300	NUM
eurjchem-289	67	3	°	°	SYM
eurjchem-289	67	4	c	c	NOUN
eurjchem-289	67	5	.	.	PUNCT
eurjchem-289	68	1	method	method	PROPN
eurjchem-289	68	2	b	b	NOUN
eurjchem-289	68	3	:	:	PUNCT
eurjchem-289	68	4	a	a	DET
eurjchem-289	68	5	mixture	mixture	NOUN
eurjchem-289	68	6	of	of	ADP
eurjchem-289	68	7	2	2	NUM
eurjchem-289	68	8	(	(	PUNCT
eurjchem-289	68	9	1.01	1.01	NUM
eurjchem-289	68	10	g	g	NOUN
eurjchem-289	68	11	,	,	PUNCT
eurjchem-289	68	12	0.005	0.005	NUM
eurjchem-289	68	13	mol	mol	NOUN
eurjchem-289	68	14	)	)	PUNCT
eurjchem-289	68	15	and	and	CCONJ
eurjchem-289	68	16	benzaldehyde	benzaldehyde	NOUN
eurjchem-289	68	17	(	(	PUNCT
eurjchem-289	68	18	0.53	0.53	NUM
eurjchem-289	68	19	g	g	NOUN
eurjchem-289	68	20	,	,	PUNCT
eurjchem-289	68	21	0.005	0.005	NUM
eurjchem-289	68	22	mol	mol	NOUN
eurjchem-289	68	23	)	)	PUNCT
eurjchem-289	68	24	was	be	AUX
eurjchem-289	68	25	heated	heat	VERB
eurjchem-289	68	26	at	at	ADP
eurjchem-289	68	27	180‐190	180‐190	NUM
eurjchem-289	68	28	°	°	PROPN
eurjchem-289	68	29	c	c	NOUN
eurjchem-289	68	30	for	for	ADP
eurjchem-289	68	31	2	2	NUM
eurjchem-289	68	32	h.	h.	NOUN
eurjchem-289	68	33	the	the	DET
eurjchem-289	68	34	solid	solid	ADJ
eurjchem-289	68	35	was	be	AUX
eurjchem-289	68	36	then	then	ADV
eurjchem-289	68	37	washed	wash	VERB
eurjchem-289	68	38	with	with	ADP
eurjchem-289	68	39	ethanol	ethanol	NOUN
eurjchem-289	68	40	and	and	CCONJ
eurjchem-289	68	41	crystallized	crystallize	VERB
eurjchem-289	68	42	from	from	ADP
eurjchem-289	68	43	ethanol	ethanol	NOUN
eurjchem-289	68	44	.	.	PUNCT
eurjchem-289	69	1	yield	yield	NOUN
eurjchem-289	69	2	:	:	PUNCT
eurjchem-289	69	3	70	70	NUM
eurjchem-289	69	4	%	%	NOUN
eurjchem-289	69	5	.	.	PUNCT
eurjchem-289	70	1	m.p	m.p	PROPN
eurjchem-289	70	2	.	.	PROPN
eurjchem-289	70	3	:	:	PUNCT
eurjchem-289	71	1	>	>	PUNCT
eurjchem-289	71	2	300	300	NUM
eurjchem-289	71	3	°	°	PRON
eurjchem-289	71	4	c	c	NOUN
eurjchem-289	71	5	[	[	X
eurjchem-289	71	6	26	26	NUM
eurjchem-289	71	7	]	]	PUNCT
eurjchem-289	71	8	.	.	PUNCT
eurjchem-289	72	1	method	method	PROPN
eurjchem-289	72	2	c	c	NOUN
eurjchem-289	72	3	:	:	PUNCT
eurjchem-289	72	4	to	to	ADP
eurjchem-289	72	5	a	a	DET
eurjchem-289	72	6	stirred	stir	VERB
eurjchem-289	72	7	solution	solution	NOUN
eurjchem-289	72	8	of	of	ADP
eurjchem-289	72	9	3a	3a	NUM
eurjchem-289	72	10	(	(	PUNCT
eurjchem-289	72	11	1.45	1.45	NUM
eurjchem-289	72	12	g	g	NOUN
eurjchem-289	72	13	,	,	PUNCT
eurjchem-289	72	14	0.005	0.005	NUM
eurjchem-289	72	15	mol	mol	NOUN
eurjchem-289	72	16	)	)	PUNCT
eurjchem-289	72	17	and	and	CCONJ
eurjchem-289	72	18	sodium	sodium	NOUN
eurjchem-289	72	19	acetate	acetate	NOUN
eurjchem-289	72	20	(	(	PUNCT
eurjchem-289	72	21	0.82	0.82	NUM
eurjchem-289	72	22	g	g	NOUN
eurjchem-289	72	23	,	,	PUNCT
eurjchem-289	72	24	0.01	0.01	NUM
eurjchem-289	72	25	mol	mol	NOUN
eurjchem-289	72	26	)	)	PUNCT
eurjchem-289	72	27	in	in	ADP
eurjchem-289	72	28	acetic	acetic	ADJ
eurjchem-289	72	29	acid	acid	NOUN
eurjchem-289	72	30	(	(	PUNCT
eurjchem-289	72	31	10	10	NUM
eurjchem-289	72	32	ml	ml	NOUN
eurjchem-289	72	33	)	)	PUNCT
eurjchem-289	72	34	,	,	PUNCT
eurjchem-289	72	35	bromine	bromine	NOUN
eurjchem-289	72	36	(	(	PUNCT
eurjchem-289	72	37	0.8	0.8	NUM
eurjchem-289	72	38	g	g	NOUN
eurjchem-289	72	39	,	,	PUNCT
eurjchem-289	72	40	0.005	0.005	NUM
eurjchem-289	72	41	mol	mol	NOUN
eurjchem-289	72	42	)	)	PUNCT
eurjchem-289	72	43	in	in	ADP
eurjchem-289	72	44	acetic	acetic	ADJ
eurjchem-289	72	45	acid	acid	NOUN
eurjchem-289	72	46	(	(	PUNCT
eurjchem-289	72	47	2.3	2.3	NUM
eurjchem-289	72	48	ml	ml	NOUN
eurjchem-289	72	49	)	)	PUNCT
eurjchem-289	72	50	was	be	AUX
eurjchem-289	72	51	added	add	VERB
eurjchem-289	72	52	dropwise	dropwise	NOUN
eurjchem-289	72	53	.	.	PUNCT
eurjchem-289	73	1	the	the	DET
eurjchem-289	73	2	reaction	reaction	NOUN
eurjchem-289	73	3	mixture	mixture	NOUN
eurjchem-289	73	4	was	be	AUX
eurjchem-289	73	5	heated	heat	VERB
eurjchem-289	73	6	under	under	ADP
eurjchem-289	73	7	reflux	reflux	NOUN
eurjchem-289	73	8	for	for	ADP
eurjchem-289	73	9	7	7	NUM
eurjchem-289	73	10	h.	h.	PROPN
eurjchem-289	73	11	water	water	NOUN
eurjchem-289	73	12	(	(	PUNCT
eurjchem-289	73	13	20	20	NUM
eurjchem-289	73	14	ml	ml	NOUN
eurjchem-289	73	15	)	)	PUNCT
eurjchem-289	73	16	was	be	AUX
eurjchem-289	73	17	then	then	ADV
eurjchem-289	73	18	added	add	VERB
eurjchem-289	73	19	and	and	CCONJ
eurjchem-289	73	20	the	the	DET
eurjchem-289	73	21	solid	solid	ADJ
eurjchem-289	73	22	product	product	NOUN
eurjchem-289	73	23	separated	separate	VERB
eurjchem-289	73	24	was	be	AUX
eurjchem-289	73	25	filtered	filter	VERB
eurjchem-289	73	26	and	and	CCONJ
eurjchem-289	73	27	crystallized	crystallize	VERB
eurjchem-289	73	28	from	from	ADP
eurjchem-289	73	29	ethanol	ethanol	NOUN
eurjchem-289	73	30	.	.	PUNCT
eurjchem-289	74	1	yield	yield	NOUN
eurjchem-289	74	2	:	:	PUNCT
eurjchem-289	74	3	60	60	NUM
eurjchem-289	74	4	%	%	NOUN
eurjchem-289	74	5	.	.	PUNCT
eurjchem-289	75	1	m.p	m.p	PROPN
eurjchem-289	75	2	.	.	PROPN
eurjchem-289	75	3	:	:	PUNCT
eurjchem-289	76	1	>	>	PUNCT
eurjchem-289	76	2	300	300	NUM
eurjchem-289	76	3	°	°	SYM
eurjchem-289	76	4	c	c	NOUN
eurjchem-289	76	5	.	.	PUNCT
eurjchem-289	77	1	shabaan	shabaan	PROPN
eurjchem-289	77	2	et	et	PROPN
eurjchem-289	77	3	al	al	PROPN
eurjchem-289	77	4	.	.	PUNCT
eurjchem-289	77	5	/	/	SYM
eurjchem-289	77	6	european	european	PROPN
eurjchem-289	77	7	journal	journal	PROPN
eurjchem-289	77	8	of	of	ADP
eurjchem-289	77	9	chemistry	chemistry	NOUN
eurjchem-289	77	10	2	2	NUM
eurjchem-289	77	11	(	(	PUNCT
eurjchem-289	77	12	3	3	NUM
eurjchem-289	77	13	)	)	PUNCT
eurjchem-289	77	14	(	(	PUNCT
eurjchem-289	77	15	2011	2011	NUM
eurjchem-289	77	16	)	)	PUNCT
eurjchem-289	77	17	365‐371	365‐371	PROPN
eurjchem-289	77	18	367	367	NUM
eurjchem-289	77	19	method	method	NOUN
eurjchem-289	77	20	d	d	NOUN
eurjchem-289	77	21	:	:	PUNCT
eurjchem-289	77	22	a	a	DET
eurjchem-289	77	23	solution	solution	NOUN
eurjchem-289	77	24	of	of	ADP
eurjchem-289	77	25	3a	3a	NUM
eurjchem-289	77	26	(	(	PUNCT
eurjchem-289	77	27	1.45	1.45	NUM
eurjchem-289	77	28	g	g	NOUN
eurjchem-289	77	29	,	,	PUNCT
eurjchem-289	77	30	0.005	0.005	NUM
eurjchem-289	77	31	mol	mol	NOUN
eurjchem-289	77	32	)	)	PUNCT
eurjchem-289	77	33	in	in	ADP
eurjchem-289	77	34	ethylene	ethylene	NOUN
eurjchem-289	77	35	glycol	glycol	NOUN
eurjchem-289	77	36	(	(	PUNCT
eurjchem-289	77	37	5	5	NUM
eurjchem-289	77	38	ml	ml	NOUN
eurjchem-289	77	39	)	)	PUNCT
eurjchem-289	77	40	was	be	AUX
eurjchem-289	77	41	heated	heat	VERB
eurjchem-289	77	42	under	under	ADP
eurjchem-289	77	43	reflux	reflux	NOUN
eurjchem-289	77	44	for	for	ADP
eurjchem-289	77	45	6	6	NUM
eurjchem-289	77	46	h.	h.	NOUN
eurjchem-289	77	47	the	the	DET
eurjchem-289	77	48	mixture	mixture	NOUN
eurjchem-289	77	49	was	be	AUX
eurjchem-289	77	50	cooled	cool	VERB
eurjchem-289	77	51	to	to	ADP
eurjchem-289	77	52	room	room	NOUN
eurjchem-289	77	53	temperature	temperature	NOUN
eurjchem-289	77	54	and	and	CCONJ
eurjchem-289	77	55	then	then	ADV
eurjchem-289	77	56	poured	pour	VERB
eurjchem-289	77	57	onto	onto	ADP
eurjchem-289	77	58	an	an	DET
eurjchem-289	77	59	ice‐water	ice‐water	NOUN
eurjchem-289	77	60	mixture	mixture	NOUN
eurjchem-289	77	61	.	.	PUNCT
eurjchem-289	78	1	the	the	DET
eurjchem-289	78	2	product	product	NOUN
eurjchem-289	78	3	was	be	AUX
eurjchem-289	78	4	filtered	filter	VERB
eurjchem-289	78	5	and	and	CCONJ
eurjchem-289	78	6	crystallized	crystallize	VERB
eurjchem-289	78	7	from	from	ADP
eurjchem-289	78	8	ethanol	ethanol	NOUN
eurjchem-289	78	9	.	.	PUNCT
eurjchem-289	79	1	yield	yield	NOUN
eurjchem-289	79	2	:	:	PUNCT
eurjchem-289	79	3	70	70	NUM
eurjchem-289	79	4	%	%	NOUN
eurjchem-289	79	5	.	.	PUNCT
eurjchem-289	80	1	m.p	m.p	PROPN
eurjchem-289	80	2	.	.	PROPN
eurjchem-289	80	3	:	:	PUNCT
eurjchem-289	81	1	>	>	PUNCT
eurjchem-289	81	2	300	300	NUM
eurjchem-289	81	3	°	°	NOUN
eurjchem-289	81	4	c	c	NOUN
eurjchem-289	81	5	.	.	PUNCT
eurjchem-289	82	1	ir	ir	PROPN
eurjchem-289	82	2	(	(	PUNCT
eurjchem-289	82	3	kbr	kbr	PROPN
eurjchem-289	82	4	,	,	PUNCT
eurjchem-289	82	5	cm‐1	cm‐1	PROPN
eurjchem-289	82	6	):	):	PUNCT
eurjchem-289	82	7	3249	3249	NUM
eurjchem-289	82	8	(	(	PUNCT
eurjchem-289	82	9	nh	nh	NOUN
eurjchem-289	82	10	)	)	PUNCT
eurjchem-289	82	11	,	,	PUNCT
eurjchem-289	82	12	1660	1660	NUM
eurjchem-289	82	13	,	,	PUNCT
eurjchem-289	82	14	1620	1620	NUM
eurjchem-289	82	15	(	(	PUNCT
eurjchem-289	82	16	c	c	NOUN
eurjchem-289	82	17	=	=	NOUN
eurjchem-289	82	18	o	o	NOUN
eurjchem-289	82	19	)	)	PUNCT
eurjchem-289	82	20	.	.	PUNCT
eurjchem-289	83	1	1h	1h	NUM
eurjchem-289	83	2	nmr	nmr	NOUN
eurjchem-289	83	3	(	(	PUNCT
eurjchem-289	83	4	chcl3	chcl3	PROPN
eurjchem-289	83	5	/	/	SYM
eurjchem-289	83	6	tfa	tfa	PROPN
eurjchem-289	83	7	,	,	PUNCT
eurjchem-289	83	8	(	(	PUNCT
eurjchem-289	83	9	5:1	5:1	NUM
eurjchem-289	83	10	)	)	PUNCT
eurjchem-289	83	11	,	,	PUNCT
eurjchem-289	83	12	δ	δ	PROPN
eurjchem-289	83	13	,	,	PUNCT
eurjchem-289	83	14	ppm	ppm	NUM
eurjchem-289	83	15	):	):	PUNCT
eurjchem-289	83	16	6.94‐	6.94‐	NUM
eurjchem-289	83	17	7.58	7.58	NUM
eurjchem-289	83	18	(	(	PUNCT
eurjchem-289	83	19	m	m	PROPN
eurjchem-289	83	20	,	,	PUNCT
eurjchem-289	83	21	11h	11h	NUM
eurjchem-289	83	22	)	)	PUNCT
eurjchem-289	83	23	.	.	PUNCT
eurjchem-289	84	1	ms	ms	NOUN
eurjchem-289	84	2	(	(	PUNCT
eurjchem-289	84	3	m	m	PROPN
eurjchem-289	84	4	/	/	SYM
eurjchem-289	84	5	z	z	NOUN
eurjchem-289	84	6	(	(	PUNCT
eurjchem-289	84	7	%	%	NOUN
eurjchem-289	84	8	)	)	PUNCT
eurjchem-289	84	9	):	):	PUNCT
eurjchem-289	84	10	288	288	NUM
eurjchem-289	84	11	(	(	PUNCT
eurjchem-289	84	12	m+	m+	NUM
eurjchem-289	84	13	.	.	PROPN
eurjchem-289	84	14	,	,	PUNCT
eurjchem-289	84	15	100	100	NUM
eurjchem-289	84	16	%	%	NOUN
eurjchem-289	84	17	)	)	PUNCT
eurjchem-289	84	18	,	,	PUNCT
eurjchem-289	84	19	289	289	NUM
eurjchem-289	84	20	(	(	PUNCT
eurjchem-289	84	21	m+1	m+1	X
eurjchem-289	84	22	┐	┐	NUM
eurjchem-289	84	23	+	+	NOUN
eurjchem-289	84	24	.	.	PROPN
eurjchem-289	84	25	,	,	PUNCT
eurjchem-289	84	26	27.01	27.01	NUM
eurjchem-289	84	27	%	%	NOUN
eurjchem-289	84	28	)	)	PUNCT
eurjchem-289	84	29	.	.	PUNCT
eurjchem-289	85	1	anal	anal	PROPN
eurjchem-289	85	2	.	.	PUNCT
eurjchem-289	85	3	calcd	calcd	NOUN
eurjchem-289	85	4	.	.	PUNCT
eurjchem-289	86	1	for	for	ADP
eurjchem-289	86	2	c18h12n2o2	c18h12n2o2	NOUN
eurjchem-289	86	3	(	(	PUNCT
eurjchem-289	86	4	288	288	NUM
eurjchem-289	86	5	):	):	PUNCT
eurjchem-289	86	6	c	c	X
eurjchem-289	86	7	,	,	PUNCT
eurjchem-289	86	8	75.00	75.00	NUM
eurjchem-289	86	9	;	;	PUNCT
eurjchem-289	86	10	h	h	X
eurjchem-289	86	11	,	,	PUNCT
eurjchem-289	86	12	4.17	4.17	NUM
eurjchem-289	86	13	;	;	PUNCT
eurjchem-289	86	14	n	n	CCONJ
eurjchem-289	86	15	,	,	PUNCT
eurjchem-289	86	16	9.72	9.72	NUM
eurjchem-289	86	17	.	.	PUNCT
eurjchem-289	86	18	found	find	VERB
eurjchem-289	86	19	:	:	PUNCT
eurjchem-289	87	1	c	c	X
eurjchem-289	87	2	,	,	PUNCT
eurjchem-289	87	3	74.95	74.95	NUM
eurjchem-289	87	4	;	;	PUNCT
eurjchem-289	87	5	h	h	NOUN
eurjchem-289	87	6	,	,	PUNCT
eurjchem-289	87	7	3.80	3.80	NUM
eurjchem-289	87	8	;	;	PUNCT
eurjchem-289	87	9	n	n	CCONJ
eurjchem-289	87	10	,	,	PUNCT
eurjchem-289	87	11	9.92	9.92	NUM
eurjchem-289	87	12	%	%	NOUN
eurjchem-289	87	13	.	.	PUNCT
eurjchem-289	88	1	2.2.4	2.2.4	NUM
eurjchem-289	88	2	.	.	X
eurjchem-289	88	3	3[(4‐aryl‐5‐cyano‐6‐oxo‐1,6‐dihydropyridin‐2‐yl	3[(4‐aryl‐5‐cyano‐6‐oxo‐1,6‐dihydropyridin‐2‐yl	NUM
eurjchem-289	88	4	)	)	PUNCT
eurjchem-289	88	5	methyl]quinoxalin‐2(1h)‐ones	methyl]quinoxalin‐2(1h)‐one	NOUN
eurjchem-289	88	6	(	(	PUNCT
eurjchem-289	88	7	5a	5a	NUM
eurjchem-289	88	8	,	,	PUNCT
eurjchem-289	88	9	b	b	NOUN
eurjchem-289	88	10	)	)	PUNCT
eurjchem-289	88	11	method	method	NOUN
eurjchem-289	88	12	a	a	PRON
eurjchem-289	88	13	:	:	PUNCT
eurjchem-289	88	14	a	a	DET
eurjchem-289	88	15	mixture	mixture	NOUN
eurjchem-289	88	16	of	of	ADP
eurjchem-289	88	17	2	2	NUM
eurjchem-289	88	18	(	(	PUNCT
eurjchem-289	88	19	1.01	1.01	NUM
eurjchem-289	88	20	g	g	NOUN
eurjchem-289	88	21	,	,	PUNCT
eurjchem-289	88	22	0.005	0.005	NUM
eurjchem-289	88	23	mol	mol	NOUN
eurjchem-289	88	24	)	)	PUNCT
eurjchem-289	88	25	,	,	PUNCT
eurjchem-289	88	26	the	the	DET
eurjchem-289	88	27	appropriate	appropriate	ADJ
eurjchem-289	88	28	aldehyde	aldehyde	NOUN
eurjchem-289	88	29	(	(	PUNCT
eurjchem-289	88	30	0.005	0.005	NUM
eurjchem-289	88	31	mol	mol	NOUN
eurjchem-289	88	32	)	)	PUNCT
eurjchem-289	88	33	,	,	PUNCT
eurjchem-289	88	34	ethyl	ethyl	PROPN
eurjchem-289	88	35	cyanoacetate	cyanoacetate	NOUN
eurjchem-289	88	36	(	(	PUNCT
eurjchem-289	88	37	0.56	0.56	NUM
eurjchem-289	88	38	g	g	NOUN
eurjchem-289	88	39	,	,	PUNCT
eurjchem-289	88	40	0.005	0.005	NUM
eurjchem-289	88	41	mol	mol	NOUN
eurjchem-289	88	42	)	)	PUNCT
eurjchem-289	88	43	and	and	CCONJ
eurjchem-289	88	44	ammonium	ammonium	NOUN
eurjchem-289	88	45	acetate	acetate	NOUN
eurjchem-289	88	46	(	(	PUNCT
eurjchem-289	88	47	3.08	3.08	NUM
eurjchem-289	88	48	g	g	NOUN
eurjchem-289	88	49	,	,	PUNCT
eurjchem-289	88	50	0.04	0.04	NUM
eurjchem-289	88	51	mol	mol	NOUN
eurjchem-289	88	52	)	)	PUNCT
eurjchem-289	88	53	in	in	ADP
eurjchem-289	88	54	absolute	absolute	ADJ
eurjchem-289	88	55	ethanol	ethanol	NOUN
eurjchem-289	88	56	(	(	PUNCT
eurjchem-289	88	57	10	10	NUM
eurjchem-289	88	58	ml	ml	NOUN
eurjchem-289	88	59	)	)	PUNCT
eurjchem-289	88	60	or	or	CCONJ
eurjchem-289	88	61	n‐butanol	n‐butanol	ADP
eurjchem-289	88	62	(	(	PUNCT
eurjchem-289	88	63	10	10	NUM
eurjchem-289	88	64	ml	ml	NOUN
eurjchem-289	88	65	)	)	PUNCT
eurjchem-289	88	66	was	be	AUX
eurjchem-289	88	67	heated	heat	VERB
eurjchem-289	88	68	under	under	ADP
eurjchem-289	88	69	reflux	reflux	NOUN
eurjchem-289	88	70	for	for	ADP
eurjchem-289	88	71	6	6	NUM
eurjchem-289	88	72	h.	h.	NOUN
eurjchem-289	88	73	the	the	DET
eurjchem-289	88	74	solvent	solvent	NOUN
eurjchem-289	88	75	was	be	AUX
eurjchem-289	88	76	evaporated	evaporate	VERB
eurjchem-289	88	77	under	under	ADP
eurjchem-289	88	78	reduced	reduce	VERB
eurjchem-289	88	79	pressure	pressure	NOUN
eurjchem-289	88	80	and	and	CCONJ
eurjchem-289	88	81	the	the	DET
eurjchem-289	88	82	residue	residue	NOUN
eurjchem-289	88	83	was	be	AUX
eurjchem-289	88	84	triturated	triturate	VERB
eurjchem-289	88	85	with	with	ADP
eurjchem-289	88	86	ethanol	ethanol	NOUN
eurjchem-289	88	87	,	,	PUNCT
eurjchem-289	88	88	filtered	filter	VERB
eurjchem-289	88	89	,	,	PUNCT
eurjchem-289	88	90	washed	wash	VERB
eurjchem-289	88	91	with	with	ADP
eurjchem-289	88	92	ethanol	ethanol	NOUN
eurjchem-289	88	93	and	and	CCONJ
eurjchem-289	88	94	crystallized	crystallize	VERB
eurjchem-289	88	95	from	from	ADP
eurjchem-289	88	96	acetone	acetone	NOUN
eurjchem-289	88	97	(	(	PUNCT
eurjchem-289	88	98	scheme	scheme	NOUN
eurjchem-289	88	99	1	1	NUM
eurjchem-289	88	100	)	)	PUNCT
eurjchem-289	88	101	.	.	PUNCT
eurjchem-289	89	1	method	method	PROPN
eurjchem-289	89	2	b	b	NOUN
eurjchem-289	89	3	:	:	PUNCT
eurjchem-289	89	4	a	a	DET
eurjchem-289	89	5	mixture	mixture	NOUN
eurjchem-289	89	6	of	of	ADP
eurjchem-289	89	7	the	the	DET
eurjchem-289	89	8	chalcone	chalcone	NOUN
eurjchem-289	89	9	analogue	analogue	NOUN
eurjchem-289	89	10	3a	3a	NUM
eurjchem-289	89	11	(	(	PUNCT
eurjchem-289	89	12	1.45	1.45	NUM
eurjchem-289	89	13	g	g	NOUN
eurjchem-289	89	14	,	,	PUNCT
eurjchem-289	89	15	0.005	0.005	NUM
eurjchem-289	89	16	mol	mol	NOUN
eurjchem-289	89	17	)	)	PUNCT
eurjchem-289	89	18	,	,	PUNCT
eurjchem-289	89	19	ethyl	ethyl	PROPN
eurjchem-289	89	20	cyanoacetate	cyanoacetate	NOUN
eurjchem-289	89	21	(	(	PUNCT
eurjchem-289	89	22	0.56	0.56	NUM
eurjchem-289	89	23	g	g	NOUN
eurjchem-289	89	24	,	,	PUNCT
eurjchem-289	89	25	0.005	0.005	NUM
eurjchem-289	89	26	mol	mol	NOUN
eurjchem-289	89	27	)	)	PUNCT
eurjchem-289	89	28	and	and	CCONJ
eurjchem-289	89	29	ammonium	ammonium	NOUN
eurjchem-289	89	30	acetate	acetate	NOUN
eurjchem-289	89	31	(	(	PUNCT
eurjchem-289	89	32	3.08	3.08	NUM
eurjchem-289	89	33	g	g	NOUN
eurjchem-289	89	34	,	,	PUNCT
eurjchem-289	89	35	0.04	0.04	NUM
eurjchem-289	89	36	mol	mol	NOUN
eurjchem-289	89	37	)	)	PUNCT
eurjchem-289	89	38	in	in	ADP
eurjchem-289	89	39	n‐butanol	n‐butanol	PROPN
eurjchem-289	89	40	(	(	PUNCT
eurjchem-289	89	41	10	10	NUM
eurjchem-289	89	42	ml	ml	NOUN
eurjchem-289	89	43	)	)	PUNCT
eurjchem-289	89	44	was	be	AUX
eurjchem-289	89	45	heated	heat	VERB
eurjchem-289	89	46	under	under	ADP
eurjchem-289	89	47	reflux	reflux	NOUN
eurjchem-289	89	48	for	for	ADP
eurjchem-289	89	49	10	10	NUM
eurjchem-289	89	50	h.	h.	NOUN
eurjchem-289	89	51	the	the	DET
eurjchem-289	89	52	solvent	solvent	NOUN
eurjchem-289	89	53	was	be	AUX
eurjchem-289	89	54	evaporated	evaporate	VERB
eurjchem-289	89	55	under	under	ADP
eurjchem-289	89	56	reduced	reduce	VERB
eurjchem-289	89	57	pressure	pressure	NOUN
eurjchem-289	89	58	and	and	CCONJ
eurjchem-289	89	59	the	the	DET
eurjchem-289	89	60	residue	residue	NOUN
eurjchem-289	89	61	was	be	AUX
eurjchem-289	89	62	triturated	triturate	VERB
eurjchem-289	89	63	with	with	ADP
eurjchem-289	89	64	ethanol	ethanol	NOUN
eurjchem-289	89	65	,	,	PUNCT
eurjchem-289	89	66	filtered	filter	VERB
eurjchem-289	89	67	,	,	PUNCT
eurjchem-289	89	68	washed	wash	VERB
eurjchem-289	89	69	with	with	ADP
eurjchem-289	89	70	ethanol	ethanol	NOUN
eurjchem-289	89	71	and	and	CCONJ
eurjchem-289	89	72	crystallized	crystallize	VERB
eurjchem-289	89	73	from	from	ADP
eurjchem-289	89	74	acetone	acetone	NOUN
eurjchem-289	89	75	(	(	PUNCT
eurjchem-289	89	76	scheme	scheme	NOUN
eurjchem-289	89	77	1	1	NUM
eurjchem-289	89	78	)	)	PUNCT
eurjchem-289	89	79	.	.	PUNCT
eurjchem-289	90	1	3[(4‐phenyl‐5‐cyano‐6‐oxo‐1,6‐dihydropyridin‐2‐yl)methyl	3[(4‐phenyl‐5‐cyano‐6‐oxo‐1,6‐dihydropyridin‐2‐yl)methyl	NUM
eurjchem-289	90	2	]	]	PUNCT
eurjchem-289	90	3	quinoxalin‐2(1h)‐ones	quinoxalin‐2(1h)‐one	NOUN
eurjchem-289	90	4	(	(	PUNCT
eurjchem-289	90	5	5a	5a	NUM
eurjchem-289	90	6	):	):	PUNCT
eurjchem-289	90	7	yield	yield	NOUN
eurjchem-289	90	8	:	:	PUNCT
eurjchem-289	90	9	68	68	NUM
eurjchem-289	90	10	%	%	NOUN
eurjchem-289	90	11	(	(	PUNCT
eurjchem-289	90	12	method	method	NOUN
eurjchem-289	90	13	a	a	PRON
eurjchem-289	90	14	)	)	PUNCT
eurjchem-289	90	15	,	,	PUNCT
eurjchem-289	90	16	77	77	NUM
eurjchem-289	90	17	%	%	NOUN
eurjchem-289	90	18	(	(	PUNCT
eurjchem-289	90	19	method	method	PROPN
eurjchem-289	90	20	b	b	NOUN
eurjchem-289	90	21	)	)	PUNCT
eurjchem-289	90	22	.	.	PUNCT
eurjchem-289	91	1	m.p	m.p	PROPN
eurjchem-289	91	2	.	.	PROPN
eurjchem-289	91	3	:	:	PUNCT
eurjchem-289	92	1	276‐278	276‐278	NUM
eurjchem-289	92	2	οc	οc	NOUN
eurjchem-289	92	3	.	.	PROPN
eurjchem-289	92	4	ir	ir	PROPN
eurjchem-289	92	5	(	(	PUNCT
eurjchem-289	92	6	kbr	kbr	PROPN
eurjchem-289	92	7	,	,	PUNCT
eurjchem-289	92	8	cm‐1	cm‐1	PROPN
eurjchem-289	92	9	):	):	PUNCT
eurjchem-289	92	10	3450	3450	NUM
eurjchem-289	92	11	,	,	PUNCT
eurjchem-289	92	12	3200	3200	NUM
eurjchem-289	92	13	(	(	PUNCT
eurjchem-289	92	14	nh	nh	NOUN
eurjchem-289	92	15	)	)	PUNCT
eurjchem-289	92	16	,	,	PUNCT
eurjchem-289	92	17	1690	1690	NUM
eurjchem-289	92	18	,	,	PUNCT
eurjchem-289	92	19	1660	1660	NUM
eurjchem-289	92	20	(	(	PUNCT
eurjchem-289	92	21	c	c	NOUN
eurjchem-289	92	22	=	=	NOUN
eurjchem-289	92	23	o	o	NOUN
eurjchem-289	92	24	)	)	PUNCT
eurjchem-289	92	25	,	,	PUNCT
eurjchem-289	92	26	2200	2200	NUM
eurjchem-289	92	27	(	(	PUNCT
eurjchem-289	92	28	cn	cn	NOUN
eurjchem-289	92	29	)	)	PUNCT
eurjchem-289	92	30	.	.	PUNCT
eurjchem-289	93	1	1h	1h	NUM
eurjchem-289	93	2	nmr	nmr	NOUN
eurjchem-289	93	3	(	(	PUNCT
eurjchem-289	93	4	dmso‐d6	dmso‐d6	PROPN
eurjchem-289	93	5	,	,	PUNCT
eurjchem-289	93	6	δ	δ	PROPN
eurjchem-289	93	7	,	,	PUNCT
eurjchem-289	93	8	ppm	ppm	NUM
eurjchem-289	93	9	):	):	PUNCT
eurjchem-289	93	10	3.42	3.42	NUM
eurjchem-289	93	11	(	(	PUNCT
eurjchem-289	93	12	s	s	PROPN
eurjchem-289	93	13	,	,	PUNCT
eurjchem-289	93	14	2h	2h	NUM
eurjchem-289	93	15	,	,	PUNCT
eurjchem-289	93	16	ch2	ch2	PROPN
eurjchem-289	93	17	)	)	PUNCT
eurjchem-289	93	18	,	,	PUNCT
eurjchem-289	93	19	7.18‐7.48	7.18‐7.48	NUM
eurjchem-289	93	20	(	(	PUNCT
eurjchem-289	93	21	m	m	PROPN
eurjchem-289	93	22	,	,	PUNCT
eurjchem-289	93	23	10h	10h	NUM
eurjchem-289	93	24	,	,	PUNCT
eurjchem-289	93	25	aromatic	aromatic	ADJ
eurjchem-289	93	26	protons	proton	NOUN
eurjchem-289	93	27	)	)	PUNCT
eurjchem-289	93	28	,	,	PUNCT
eurjchem-289	93	29	12.14	12.14	NUM
eurjchem-289	93	30	(	(	PUNCT
eurjchem-289	93	31	br	br	PROPN
eurjchem-289	93	32	,	,	PUNCT
eurjchem-289	93	33	2h	2h	NUM
eurjchem-289	93	34	,	,	PUNCT
eurjchem-289	93	35	2nh	2nh	NOUN
eurjchem-289	93	36	,	,	PUNCT
eurjchem-289	93	37	exchanged	exchange	VERB
eurjchem-289	93	38	with	with	ADP
eurjchem-289	93	39	d2o	d2o	NOUN
eurjchem-289	93	40	)	)	PUNCT
eurjchem-289	93	41	.	.	PUNCT
eurjchem-289	94	1	ms	ms	NOUN
eurjchem-289	94	2	(	(	PUNCT
eurjchem-289	94	3	m	m	PROPN
eurjchem-289	94	4	/	/	SYM
eurjchem-289	94	5	z	z	NOUN
eurjchem-289	94	6	(	(	PUNCT
eurjchem-289	94	7	%	%	NOUN
eurjchem-289	94	8	)	)	PUNCT
eurjchem-289	94	9	):	):	PUNCT
eurjchem-289	94	10	251	251	NUM
eurjchem-289	94	11	(	(	PUNCT
eurjchem-289	94	12	100	100	NUM
eurjchem-289	94	13	%	%	NOUN
eurjchem-289	94	14	)	)	PUNCT
eurjchem-289	94	15	,	,	PUNCT
eurjchem-289	94	16	354	354	NUM
eurjchem-289	94	17	(	(	PUNCT
eurjchem-289	94	18	m+	m+	NUM
eurjchem-289	94	19	.	.	PROPN
eurjchem-289	94	20	,	,	PUNCT
eurjchem-289	94	21	0.28	0.28	NUM
eurjchem-289	94	22	%	%	NOUN
eurjchem-289	94	23	)	)	PUNCT
eurjchem-289	94	24	.	.	PUNCT
eurjchem-289	95	1	anal	anal	PROPN
eurjchem-289	95	2	.	.	PUNCT
eurjchem-289	95	3	calcd	calcd	NOUN
eurjchem-289	95	4	.	.	PUNCT
eurjchem-289	96	1	for	for	ADP
eurjchem-289	96	2	c21h14n4o2	c21h14n4o2	PROPN
eurjchem-289	96	3	(	(	PUNCT
eurjchem-289	96	4	354	354	NUM
eurjchem-289	96	5	):	):	PUNCT
eurjchem-289	96	6	c	c	NOUN
eurjchem-289	96	7	,	,	PUNCT
eurjchem-289	96	8	71.18	71.18	NUM
eurjchem-289	96	9	;	;	PUNCT
eurjchem-289	96	10	h	h	NOUN
eurjchem-289	96	11	,	,	PUNCT
eurjchem-289	96	12	3.95	3.95	NUM
eurjchem-289	96	13	;	;	PUNCT
eurjchem-289	96	14	n	n	CCONJ
eurjchem-289	96	15	,	,	PUNCT
eurjchem-289	96	16	15.81	15.81	NUM
eurjchem-289	96	17	.	.	PUNCT
eurjchem-289	97	1	found	find	VERB
eurjchem-289	97	2	:	:	PUNCT
eurjchem-289	98	1	c	c	X
eurjchem-289	98	2	,	,	PUNCT
eurjchem-289	98	3	70.80	70.80	NUM
eurjchem-289	98	4	;	;	PUNCT
eurjchem-289	98	5	h	h	NOUN
eurjchem-289	98	6	,	,	PUNCT
eurjchem-289	98	7	4.20	4.20	NUM
eurjchem-289	98	8	;	;	PUNCT
eurjchem-289	98	9	n	n	CCONJ
eurjchem-289	98	10	,	,	PUNCT
eurjchem-289	98	11	15.72	15.72	NUM
eurjchem-289	98	12	%	%	NOUN
eurjchem-289	98	13	.	.	PUNCT
eurjchem-289	99	1	3[(4‐(3‐nitrophenyl)‐5‐cyano‐6‐oxo‐1,6‐dihydropyridin‐2‐	3[(4‐(3‐nitrophenyl)‐5‐cyano‐6‐oxo‐1,6‐dihydropyridin‐2‐	NUM
eurjchem-289	99	2	yl)methyl]quinoxalin‐2(1h)‐ones	yl)methyl]quinoxalin‐2(1h)‐one	NOUN
eurjchem-289	99	3	(	(	PUNCT
eurjchem-289	99	4	5b	5b	NUM
eurjchem-289	99	5	):	):	PUNCT
eurjchem-289	99	6	yield	yield	NOUN
eurjchem-289	99	7	:	:	PUNCT
eurjchem-289	99	8	51	51	NUM
eurjchem-289	99	9	%	%	NOUN
eurjchem-289	99	10	(	(	PUNCT
eurjchem-289	99	11	method	method	NOUN
eurjchem-289	99	12	a	a	PRON
eurjchem-289	99	13	)	)	PUNCT
eurjchem-289	99	14	.	.	PUNCT
eurjchem-289	100	1	m.p	m.p	PROPN
eurjchem-289	100	2	.	.	PROPN
eurjchem-289	100	3	:	:	PUNCT
eurjchem-289	101	1	292‐294	292‐294	NUM
eurjchem-289	101	2	οc	οc	ADV
eurjchem-289	101	3	.	.	PROPN
eurjchem-289	102	1	ir	ir	PROPN
eurjchem-289	102	2	(	(	PUNCT
eurjchem-289	102	3	kbr	kbr	PROPN
eurjchem-289	102	4	,	,	PUNCT
eurjchem-289	102	5	cm‐1	cm‐1	PROPN
eurjchem-289	102	6	):	):	PUNCT
eurjchem-289	102	7	3450	3450	NUM
eurjchem-289	102	8	,	,	PUNCT
eurjchem-289	102	9	3350	3350	NUM
eurjchem-289	102	10	(	(	PUNCT
eurjchem-289	102	11	nh	nh	NOUN
eurjchem-289	102	12	)	)	PUNCT
eurjchem-289	102	13	,	,	PUNCT
eurjchem-289	102	14	1690	1690	NUM
eurjchem-289	102	15	,	,	PUNCT
eurjchem-289	102	16	1670	1670	NUM
eurjchem-289	102	17	(	(	PUNCT
eurjchem-289	102	18	c	c	NOUN
eurjchem-289	102	19	=	=	NOUN
eurjchem-289	102	20	o	o	NOUN
eurjchem-289	102	21	)	)	PUNCT
eurjchem-289	102	22	,	,	PUNCT
eurjchem-289	102	23	2200	2200	NUM
eurjchem-289	102	24	(	(	PUNCT
eurjchem-289	102	25	cn	cn	NOUN
eurjchem-289	102	26	)	)	PUNCT
eurjchem-289	102	27	.	.	PUNCT
eurjchem-289	103	1	1h	1h	NUM
eurjchem-289	103	2	nmr	nmr	NOUN
eurjchem-289	103	3	(	(	PUNCT
eurjchem-289	103	4	dmso‐d6	dmso‐d6	PROPN
eurjchem-289	103	5	,	,	PUNCT
eurjchem-289	103	6	δ	δ	PROPN
eurjchem-289	103	7	,	,	PUNCT
eurjchem-289	103	8	ppm	ppm	NUM
eurjchem-289	103	9	):	):	PUNCT
eurjchem-289	103	10	3.31	3.31	NUM
eurjchem-289	103	11	(	(	PUNCT
eurjchem-289	103	12	s	s	PROPN
eurjchem-289	103	13	,	,	PUNCT
eurjchem-289	103	14	2h	2h	NUM
eurjchem-289	103	15	,	,	PUNCT
eurjchem-289	103	16	ch2	ch2	PROPN
eurjchem-289	103	17	)	)	PUNCT
eurjchem-289	103	18	,	,	PUNCT
eurjchem-289	103	19	7.21‐7.42	7.21‐7.42	NUM
eurjchem-289	103	20	(	(	PUNCT
eurjchem-289	103	21	m	m	PROPN
eurjchem-289	103	22	,	,	PUNCT
eurjchem-289	103	23	9h	9h	NOUN
eurjchem-289	103	24	,	,	PUNCT
eurjchem-289	103	25	aromatic	aromatic	ADJ
eurjchem-289	103	26	protons	proton	NOUN
eurjchem-289	103	27	)	)	PUNCT
eurjchem-289	103	28	,	,	PUNCT
eurjchem-289	103	29	12.11	12.11	NUM
eurjchem-289	103	30	(	(	PUNCT
eurjchem-289	103	31	br	br	PROPN
eurjchem-289	103	32	,	,	PUNCT
eurjchem-289	103	33	2h	2h	NUM
eurjchem-289	103	34	,	,	PUNCT
eurjchem-289	103	35	2nh	2nh	NOUN
eurjchem-289	103	36	,	,	PUNCT
eurjchem-289	103	37	exchanged	exchange	VERB
eurjchem-289	103	38	with	with	ADP
eurjchem-289	103	39	d2o	d2o	NOUN
eurjchem-289	103	40	)	)	PUNCT
eurjchem-289	103	41	.	.	PUNCT
eurjchem-289	104	1	anal	anal	PROPN
eurjchem-289	104	2	.	.	PUNCT
eurjchem-289	104	3	calcd	calcd	NOUN
eurjchem-289	104	4	.	.	PUNCT
eurjchem-289	105	1	for	for	SCONJ
eurjchem-289	105	2	c21h13n5o4	c21h13n5o4	PROPN
eurjchem-289	105	3	(	(	PUNCT
eurjchem-289	105	4	399	399	NUM
eurjchem-289	105	5	):	):	PUNCT
eurjchem-289	105	6	c	c	X
eurjchem-289	105	7	,	,	PUNCT
eurjchem-289	105	8	63.16	63.16	NUM
eurjchem-289	105	9	;	;	PUNCT
eurjchem-289	105	10	h	h	X
eurjchem-289	105	11	,	,	PUNCT
eurjchem-289	105	12	3.25	3.25	NUM
eurjchem-289	105	13	;	;	PUNCT
eurjchem-289	105	14	n	n	CCONJ
eurjchem-289	105	15	,	,	PUNCT
eurjchem-289	105	16	17.54	17.54	NUM
eurjchem-289	105	17	.	.	PUNCT
eurjchem-289	105	18	found	find	VERB
eurjchem-289	105	19	:	:	PUNCT
eurjchem-289	106	1	c	c	X
eurjchem-289	106	2	,	,	PUNCT
eurjchem-289	106	3	63.42	63.42	NUM
eurjchem-289	106	4	;	;	PUNCT
eurjchem-289	106	5	h	h	NOUN
eurjchem-289	106	6	,	,	PUNCT
eurjchem-289	106	7	3.57	3.57	NUM
eurjchem-289	106	8	;	;	PUNCT
eurjchem-289	106	9	n	n	CCONJ
eurjchem-289	106	10	,	,	PUNCT
eurjchem-289	106	11	17.25	17.25	NUM
eurjchem-289	106	12	%	%	NOUN
eurjchem-289	106	13	.	.	PUNCT
eurjchem-289	107	1	2.2.5	2.2.5	NUM
eurjchem-289	107	2	.	.	X
eurjchem-289	108	1	3[(4‐aryl‐5‐cyano‐6‐amino‐1‐pyridin‐2‐yl)methyl	3[(4‐aryl‐5‐cyano‐6‐amino‐1‐pyridin‐2‐yl)methyl	NUM
eurjchem-289	108	2	]	]	PUNCT
eurjchem-289	108	3	quinoxlin‐2(1h)‐ones	quinoxlin‐2(1h)‐one	NOUN
eurjchem-289	108	4	(	(	PUNCT
eurjchem-289	108	5	6a‐c	6a‐c	NOUN
eurjchem-289	108	6	)	)	PUNCT
eurjchem-289	108	7	a	a	DET
eurjchem-289	108	8	mixture	mixture	NOUN
eurjchem-289	108	9	of	of	ADP
eurjchem-289	108	10	2	2	NUM
eurjchem-289	108	11	(	(	PUNCT
eurjchem-289	108	12	1.01	1.01	NUM
eurjchem-289	108	13	g	g	NOUN
eurjchem-289	108	14	,	,	PUNCT
eurjchem-289	108	15	0.005	0.005	NUM
eurjchem-289	108	16	mol	mol	NOUN
eurjchem-289	108	17	)	)	PUNCT
eurjchem-289	108	18	,	,	PUNCT
eurjchem-289	108	19	the	the	DET
eurjchem-289	108	20	appropriate	appropriate	ADJ
eurjchem-289	108	21	aldehyde	aldehyde	NOUN
eurjchem-289	108	22	(	(	PUNCT
eurjchem-289	108	23	0.005	0.005	NUM
eurjchem-289	108	24	mol	mol	NOUN
eurjchem-289	108	25	)	)	PUNCT
eurjchem-289	108	26	,	,	PUNCT
eurjchem-289	108	27	malononitrile	malononitrile	NOUN
eurjchem-289	108	28	(	(	PUNCT
eurjchem-289	108	29	0.33	0.33	NUM
eurjchem-289	108	30	g	g	NOUN
eurjchem-289	108	31	,	,	PUNCT
eurjchem-289	108	32	0.005	0.005	NUM
eurjchem-289	108	33	mol	mol	NOUN
eurjchem-289	108	34	)	)	PUNCT
eurjchem-289	108	35	and	and	CCONJ
eurjchem-289	108	36	ammonium	ammonium	NOUN
eurjchem-289	108	37	acetate	acetate	NOUN
eurjchem-289	108	38	(	(	PUNCT
eurjchem-289	108	39	3.08	3.08	NUM
eurjchem-289	108	40	g	g	NOUN
eurjchem-289	108	41	,	,	PUNCT
eurjchem-289	108	42	0.04	0.04	NUM
eurjchem-289	108	43	mol	mol	NOUN
eurjchem-289	108	44	)	)	PUNCT
eurjchem-289	108	45	in	in	ADP
eurjchem-289	108	46	absolute	absolute	ADJ
eurjchem-289	108	47	ethanol	ethanol	NOUN
eurjchem-289	108	48	(	(	PUNCT
eurjchem-289	108	49	10	10	NUM
eurjchem-289	108	50	ml	ml	NOUN
eurjchem-289	108	51	)	)	PUNCT
eurjchem-289	108	52	was	be	AUX
eurjchem-289	108	53	heated	heat	VERB
eurjchem-289	108	54	under	under	ADP
eurjchem-289	108	55	reflux	reflux	NOUN
eurjchem-289	108	56	for	for	ADP
eurjchem-289	108	57	6	6	NUM
eurjchem-289	108	58	h.	h.	NOUN
eurjchem-289	108	59	the	the	DET
eurjchem-289	108	60	solvent	solvent	NOUN
eurjchem-289	108	61	was	be	AUX
eurjchem-289	108	62	evaporated	evaporate	VERB
eurjchem-289	108	63	under	under	ADP
eurjchem-289	108	64	reduced	reduce	VERB
eurjchem-289	108	65	pressure	pressure	NOUN
eurjchem-289	108	66	and	and	CCONJ
eurjchem-289	108	67	the	the	DET
eurjchem-289	108	68	residue	residue	NOUN
eurjchem-289	108	69	was	be	AUX
eurjchem-289	108	70	triturated	triturate	VERB
eurjchem-289	108	71	with	with	ADP
eurjchem-289	108	72	ethanol	ethanol	NOUN
eurjchem-289	108	73	,	,	PUNCT
eurjchem-289	108	74	filtered	filter	VERB
eurjchem-289	108	75	,	,	PUNCT
eurjchem-289	108	76	washed	wash	VERB
eurjchem-289	108	77	with	with	ADP
eurjchem-289	108	78	ethanol	ethanol	NOUN
eurjchem-289	108	79	and	and	CCONJ
eurjchem-289	108	80	crystallized	crystallize	VERB
eurjchem-289	108	81	from	from	ADP
eurjchem-289	108	82	acetone	acetone	NOUN
eurjchem-289	108	83	(	(	PUNCT
eurjchem-289	108	84	scheme	scheme	NOUN
eurjchem-289	108	85	1	1	NUM
eurjchem-289	108	86	)	)	PUNCT
eurjchem-289	108	87	.	.	PUNCT
eurjchem-289	109	1	3[(4‐phenyl‐5‐cyano‐6‐amino‐1‐pyridin‐2‐yl)methyl]quin‐	3[(4‐phenyl‐5‐cyano‐6‐amino‐1‐pyridin‐2‐yl)methyl]quin‐	NUM
eurjchem-289	109	2	oxlin‐2(1h)‐one	oxlin‐2(1h)‐one	NOUN
eurjchem-289	109	3	(	(	PUNCT
eurjchem-289	109	4	6a	6a	NOUN
eurjchem-289	109	5	):	):	PUNCT
eurjchem-289	109	6	yield	yield	NOUN
eurjchem-289	109	7	:	:	PUNCT
eurjchem-289	109	8	55	55	NUM
eurjchem-289	109	9	%	%	NOUN
eurjchem-289	109	10	.	.	PUNCT
eurjchem-289	110	1	m.p	m.p	PROPN
eurjchem-289	110	2	.	.	PROPN
eurjchem-289	110	3	:	:	PUNCT
eurjchem-289	111	1	>	>	PUNCT
eurjchem-289	111	2	300	300	NUM
eurjchem-289	111	3	οc	οc	NOUN
eurjchem-289	111	4	.	.	PROPN
eurjchem-289	111	5	ir	ir	PROPN
eurjchem-289	111	6	(	(	PUNCT
eurjchem-289	111	7	kbr	kbr	PROPN
eurjchem-289	111	8	,	,	PUNCT
eurjchem-289	111	9	cm‐1	cm‐1	PROPN
eurjchem-289	111	10	):	):	PUNCT
eurjchem-289	111	11	3350	3350	NUM
eurjchem-289	111	12	,	,	PUNCT
eurjchem-289	111	13	3200	3200	NUM
eurjchem-289	111	14	(	(	PUNCT
eurjchem-289	111	15	nh	nh	NOUN
eurjchem-289	111	16	)	)	PUNCT
eurjchem-289	111	17	,	,	PUNCT
eurjchem-289	111	18	1685	1685	NUM
eurjchem-289	111	19	(	(	PUNCT
eurjchem-289	111	20	c	c	NOUN
eurjchem-289	111	21	=	=	NOUN
eurjchem-289	111	22	o	o	NOUN
eurjchem-289	111	23	)	)	PUNCT
eurjchem-289	111	24	,	,	PUNCT
eurjchem-289	111	25	2200	2200	NUM
eurjchem-289	111	26	(	(	PUNCT
eurjchem-289	111	27	cn	cn	NOUN
eurjchem-289	111	28	)	)	PUNCT
eurjchem-289	111	29	.	.	PUNCT
eurjchem-289	112	1	1h	1h	NUM
eurjchem-289	112	2	nmr	nmr	NOUN
eurjchem-289	112	3	(	(	PUNCT
eurjchem-289	112	4	dmso‐d6	dmso‐d6	PROPN
eurjchem-289	112	5	,	,	PUNCT
eurjchem-289	112	6	δ	δ	PROPN
eurjchem-289	112	7	,	,	PUNCT
eurjchem-289	112	8	ppm	ppm	NUM
eurjchem-289	112	9	):	):	PUNCT
eurjchem-289	112	10	3.42	3.42	NUM
eurjchem-289	112	11	(	(	PUNCT
eurjchem-289	112	12	s	s	PROPN
eurjchem-289	112	13	,	,	PUNCT
eurjchem-289	112	14	2h	2h	NUM
eurjchem-289	112	15	,	,	PUNCT
eurjchem-289	112	16	ch2	ch2	PROPN
eurjchem-289	112	17	)	)	PUNCT
eurjchem-289	112	18	,	,	PUNCT
eurjchem-289	112	19	7.15‐8.15	7.15‐8.15	NUM
eurjchem-289	112	20	(	(	PUNCT
eurjchem-289	112	21	m	m	PROPN
eurjchem-289	112	22	,	,	PUNCT
eurjchem-289	112	23	10h	10h	NUM
eurjchem-289	112	24	,	,	PUNCT
eurjchem-289	112	25	aromatic	aromatic	ADJ
eurjchem-289	112	26	protons	proton	NOUN
eurjchem-289	112	27	)	)	PUNCT
eurjchem-289	112	28	,	,	PUNCT
eurjchem-289	112	29	7.74	7.74	NUM
eurjchem-289	112	30	,	,	PUNCT
eurjchem-289	112	31	7.80	7.80	NUM
eurjchem-289	112	32	and	and	CCONJ
eurjchem-289	112	33	11.80	11.80	NUM
eurjchem-289	112	34	(	(	PUNCT
eurjchem-289	112	35	s	s	PROPN
eurjchem-289	112	36	,	,	PUNCT
eurjchem-289	112	37	3h	3h	NUM
eurjchem-289	112	38	,	,	PUNCT
eurjchem-289	112	39	nh	nh	PROPN
eurjchem-289	112	40	exchanged	exchange	VERB
eurjchem-289	112	41	with	with	ADP
eurjchem-289	112	42	d2o	d2o	NOUN
eurjchem-289	112	43	)	)	PUNCT
eurjchem-289	112	44	.	.	PUNCT
eurjchem-289	113	1	ms	ms	NOUN
eurjchem-289	113	2	(	(	PUNCT
eurjchem-289	113	3	m	m	PROPN
eurjchem-289	113	4	/	/	SYM
eurjchem-289	113	5	z	z	NOUN
eurjchem-289	113	6	(	(	PUNCT
eurjchem-289	113	7	%	%	NOUN
eurjchem-289	113	8	)	)	PUNCT
eurjchem-289	113	9	):	):	PUNCT
eurjchem-289	113	10	83	83	NUM
eurjchem-289	113	11	(	(	PUNCT
eurjchem-289	113	12	100	100	NUM
eurjchem-289	113	13	%	%	NOUN
eurjchem-289	113	14	)	)	PUNCT
eurjchem-289	113	15	,	,	PUNCT
eurjchem-289	113	16	353	353	NUM
eurjchem-289	113	17	(	(	PUNCT
eurjchem-289	113	18	m+	m+	NUM
eurjchem-289	113	19	.	.	PROPN
eurjchem-289	113	20	,	,	PUNCT
eurjchem-289	113	21	7.26	7.26	NUM
eurjchem-289	113	22	%	%	NOUN
eurjchem-289	113	23	)	)	PUNCT
eurjchem-289	113	24	.	.	PUNCT
eurjchem-289	114	1	anal	anal	PROPN
eurjchem-289	114	2	.	.	PUNCT
eurjchem-289	114	3	calcd	calcd	NOUN
eurjchem-289	114	4	.	.	PUNCT
eurjchem-289	115	1	for	for	SCONJ
eurjchem-289	115	2	c21h15n5o	c21h15n5o	PROPN
eurjchem-289	115	3	(	(	PUNCT
eurjchem-289	115	4	353	353	NUM
eurjchem-289	115	5	):	):	PUNCT
eurjchem-289	115	6	c	c	X
eurjchem-289	115	7	,	,	PUNCT
eurjchem-289	115	8	71.38	71.38	NUM
eurjchem-289	115	9	;	;	PUNCT
eurjchem-289	115	10	h	h	NOUN
eurjchem-289	115	11	,	,	PUNCT
eurjchem-289	115	12	4.24	4.24	NUM
eurjchem-289	115	13	;	;	PUNCT
eurjchem-289	115	14	n	n	CCONJ
eurjchem-289	115	15	,	,	PUNCT
eurjchem-289	115	16	19.85	19.85	NUM
eurjchem-289	115	17	.	.	PUNCT
eurjchem-289	115	18	found	find	VERB
eurjchem-289	115	19	:	:	PUNCT
eurjchem-289	116	1	c	c	X
eurjchem-289	116	2	,	,	PUNCT
eurjchem-289	116	3	71.10	71.10	NUM
eurjchem-289	116	4	;	;	PUNCT
eurjchem-289	117	1	h	h	NOUN
eurjchem-289	117	2	,	,	PUNCT
eurjchem-289	117	3	4.28	4.28	NUM
eurjchem-289	117	4	;	;	PUNCT
eurjchem-289	117	5	n	n	CCONJ
eurjchem-289	117	6	,	,	PUNCT
eurjchem-289	117	7	19.79	19.79	NUM
eurjchem-289	117	8	%	%	NOUN
eurjchem-289	117	9	.	.	PUNCT
eurjchem-289	118	1	3[(4‐(4‐chlorophenyl)‐5‐cyano‐6‐amino‐1‐pyridin‐2‐yl	3[(4‐(4‐chlorophenyl)‐5‐cyano‐6‐amino‐1‐pyridin‐2‐yl	X
eurjchem-289	118	2	)	)	PUNCT
eurjchem-289	118	3	methyl]quinoxlin‐2(1h)‐one	methyl]quinoxlin‐2(1h)‐one	NOUN
eurjchem-289	118	4	(	(	PUNCT
eurjchem-289	118	5	6b	6b	NOUN
eurjchem-289	118	6	):	):	PUNCT
eurjchem-289	118	7	yield	yield	NOUN
eurjchem-289	118	8	:	:	PUNCT
eurjchem-289	118	9	60	60	NUM
eurjchem-289	118	10	%	%	NOUN
eurjchem-289	118	11	.	.	PUNCT
eurjchem-289	119	1	m.p	m.p	PROPN
eurjchem-289	119	2	.	.	PROPN
eurjchem-289	119	3	:	:	PUNCT
eurjchem-289	120	1	>	>	PUNCT
eurjchem-289	120	2	300	300	NUM
eurjchem-289	120	3	οc	οc	NOUN
eurjchem-289	120	4	.	.	PROPN
eurjchem-289	120	5	ir	ir	PROPN
eurjchem-289	120	6	(	(	PUNCT
eurjchem-289	120	7	kbr	kbr	PROPN
eurjchem-289	120	8	,	,	PUNCT
eurjchem-289	120	9	cm‐1	cm‐1	PROPN
eurjchem-289	120	10	):	):	PUNCT
eurjchem-289	120	11	3450	3450	NUM
eurjchem-289	120	12	,	,	PUNCT
eurjchem-289	120	13	3400	3400	NUM
eurjchem-289	120	14	(	(	PUNCT
eurjchem-289	120	15	nh2	nh2	PROPN
eurjchem-289	120	16	)	)	PUNCT
eurjchem-289	120	17	,	,	PUNCT
eurjchem-289	120	18	1690	1690	NUM
eurjchem-289	120	19	(	(	PUNCT
eurjchem-289	120	20	c	c	NOUN
eurjchem-289	120	21	=	=	NOUN
eurjchem-289	120	22	o	o	NOUN
eurjchem-289	120	23	)	)	PUNCT
eurjchem-289	120	24	,	,	PUNCT
eurjchem-289	120	25	2200	2200	NUM
eurjchem-289	120	26	(	(	PUNCT
eurjchem-289	120	27	cn	cn	NOUN
eurjchem-289	120	28	)	)	PUNCT
eurjchem-289	120	29	.	.	PUNCT
eurjchem-289	121	1	1h	1h	NUM
eurjchem-289	121	2	nmr	nmr	NOUN
eurjchem-289	121	3	(	(	PUNCT
eurjchem-289	121	4	dmso‐d6	dmso‐d6	PROPN
eurjchem-289	121	5	,	,	PUNCT
eurjchem-289	121	6	δ	δ	PROPN
eurjchem-289	121	7	,	,	PUNCT
eurjchem-289	121	8	ppm	ppm	NUM
eurjchem-289	121	9	):	):	PUNCT
eurjchem-289	121	10	3.47	3.47	NUM
eurjchem-289	121	11	(	(	PUNCT
eurjchem-289	121	12	s	s	PROPN
eurjchem-289	121	13	,	,	PUNCT
eurjchem-289	121	14	2h	2h	NUM
eurjchem-289	121	15	,	,	PUNCT
eurjchem-289	121	16	ch2	ch2	PROPN
eurjchem-289	121	17	)	)	PUNCT
eurjchem-289	121	18	,	,	PUNCT
eurjchem-289	121	19	7.06‐8.18	7.06‐8.18	NUM
eurjchem-289	121	20	(	(	PUNCT
eurjchem-289	121	21	m	m	PROPN
eurjchem-289	121	22	,	,	PUNCT
eurjchem-289	121	23	9h	9h	NOUN
eurjchem-289	121	24	,	,	PUNCT
eurjchem-289	121	25	aromatic	aromatic	ADJ
eurjchem-289	121	26	protons	proton	NOUN
eurjchem-289	121	27	)	)	PUNCT
eurjchem-289	121	28	,	,	PUNCT
eurjchem-289	121	29	11.00	11.00	NUM
eurjchem-289	121	30	,	,	PUNCT
eurjchem-289	121	31	11.10	11.10	NUM
eurjchem-289	121	32	and	and	CCONJ
eurjchem-289	121	33	11.76	11.76	NUM
eurjchem-289	121	34	(	(	PUNCT
eurjchem-289	121	35	s	s	PROPN
eurjchem-289	121	36	,	,	PUNCT
eurjchem-289	121	37	3h	3h	NUM
eurjchem-289	121	38	,	,	PUNCT
eurjchem-289	121	39	nh	nh	PROPN
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eurjchem-289	121	41	with	with	ADP
eurjchem-289	121	42	d2o	d2o	NOUN
eurjchem-289	121	43	)	)	PUNCT
eurjchem-289	121	44	.	.	PUNCT
eurjchem-289	122	1	anal	anal	PROPN
eurjchem-289	122	2	.	.	PUNCT
eurjchem-289	122	3	calcd	calcd	NOUN
eurjchem-289	122	4	.	.	PUNCT
eurjchem-289	123	1	for	for	ADP
eurjchem-289	123	2	c21h14cln5o	c21h14cln5o	NOUN
eurjchem-289	123	3	(	(	PUNCT
eurjchem-289	123	4	387.5	387.5	NUM
eurjchem-289	123	5	):	):	PUNCT
eurjchem-289	123	6	c	c	NOUN
eurjchem-289	123	7	,	,	PUNCT
eurjchem-289	123	8	65.03	65.03	NUM
eurjchem-289	123	9	;	;	PUNCT
eurjchem-289	123	10	h	h	NOUN
eurjchem-289	123	11	,	,	PUNCT
eurjchem-289	123	12	3.61	3.61	NUM
eurjchem-289	123	13	;	;	PUNCT
eurjchem-289	123	14	n	n	CCONJ
eurjchem-289	123	15	,	,	PUNCT
eurjchem-289	123	16	18.06	18.06	NUM
eurjchem-289	123	17	.	.	PUNCT
eurjchem-289	123	18	found	find	VERB
eurjchem-289	123	19	:	:	PUNCT
eurjchem-289	124	1	c	c	X
eurjchem-289	124	2	,	,	PUNCT
eurjchem-289	124	3	65.33	65.33	NUM
eurjchem-289	124	4	;	;	PUNCT
eurjchem-289	125	1	h	h	NOUN
eurjchem-289	125	2	,	,	PUNCT
eurjchem-289	125	3	3.62	3.62	NUM
eurjchem-289	125	4	;	;	PUNCT
eurjchem-289	125	5	n	n	CCONJ
eurjchem-289	125	6	,	,	PUNCT
eurjchem-289	125	7	17.99	17.99	NUM
eurjchem-289	125	8	%	%	NOUN
eurjchem-289	125	9	.	.	PUNCT
eurjchem-289	126	1	3[(4‐(3‐nitrophenyl)‐5‐cyano‐6‐amino‐1‐pyridin‐2‐yl	3[(4‐(3‐nitrophenyl)‐5‐cyano‐6‐amino‐1‐pyridin‐2‐yl	NUM
eurjchem-289	126	2	)	)	PUNCT
eurjchem-289	126	3	methyl]quinoxlin‐2(1h)‐one	methyl]quinoxlin‐2(1h)‐one	NOUN
eurjchem-289	126	4	(	(	PUNCT
eurjchem-289	126	5	6c	6c	NOUN
eurjchem-289	126	6	):	):	PUNCT
eurjchem-289	126	7	yield	yield	NOUN
eurjchem-289	126	8	:	:	PUNCT
eurjchem-289	126	9	50	50	NUM
eurjchem-289	126	10	%	%	NOUN
eurjchem-289	126	11	.	.	PUNCT
eurjchem-289	127	1	m.p	m.p	PROPN
eurjchem-289	127	2	.	.	PROPN
eurjchem-289	127	3	:	:	PUNCT
eurjchem-289	128	1	238‐240	238‐240	NUM
eurjchem-289	128	2	οc	οc	PROPN
eurjchem-289	128	3	.	.	PROPN
eurjchem-289	128	4	ir	ir	PROPN
eurjchem-289	128	5	(	(	PUNCT
eurjchem-289	128	6	kbr	kbr	PROPN
eurjchem-289	128	7	,	,	PUNCT
eurjchem-289	128	8	cm‐1	cm‐1	PROPN
eurjchem-289	128	9	):	):	PUNCT
eurjchem-289	128	10	3300	3300	NUM
eurjchem-289	128	11	,	,	PUNCT
eurjchem-289	128	12	3250	3250	NUM
eurjchem-289	128	13	(	(	PUNCT
eurjchem-289	128	14	nh2	nh2	PROPN
eurjchem-289	128	15	)	)	PUNCT
eurjchem-289	128	16	,	,	PUNCT
eurjchem-289	128	17	1690	1690	NUM
eurjchem-289	128	18	(	(	PUNCT
eurjchem-289	128	19	c	c	NOUN
eurjchem-289	128	20	=	=	NOUN
eurjchem-289	128	21	o	o	NOUN
eurjchem-289	128	22	)	)	PUNCT
eurjchem-289	128	23	,	,	PUNCT
eurjchem-289	128	24	2200	2200	NUM
eurjchem-289	128	25	(	(	PUNCT
eurjchem-289	128	26	cn	cn	NOUN
eurjchem-289	128	27	)	)	PUNCT
eurjchem-289	128	28	.	.	PUNCT
eurjchem-289	129	1	1h	1h	NUM
eurjchem-289	129	2	nmr	nmr	NOUN
eurjchem-289	129	3	(	(	PUNCT
eurjchem-289	129	4	dmso‐d6	dmso‐d6	PROPN
eurjchem-289	129	5	,	,	PUNCT
eurjchem-289	129	6	δ	δ	PROPN
eurjchem-289	129	7	,	,	PUNCT
eurjchem-289	129	8	ppm	ppm	NUM
eurjchem-289	129	9	):	):	PUNCT
eurjchem-289	129	10	3.90	3.90	NUM
eurjchem-289	129	11	(	(	PUNCT
eurjchem-289	129	12	s	s	PROPN
eurjchem-289	129	13	,	,	PUNCT
eurjchem-289	129	14	2h	2h	NUM
eurjchem-289	129	15	,	,	PUNCT
eurjchem-289	129	16	ch2	ch2	PROPN
eurjchem-289	129	17	)	)	PUNCT
eurjchem-289	129	18	,	,	PUNCT
eurjchem-289	129	19	7.05‐8.63	7.05‐8.63	NUM
eurjchem-289	129	20	(	(	PUNCT
eurjchem-289	129	21	m	m	PROPN
eurjchem-289	129	22	,	,	PUNCT
eurjchem-289	129	23	9h	9h	NOUN
eurjchem-289	129	24	,	,	PUNCT
eurjchem-289	129	25	aromatic	aromatic	ADJ
eurjchem-289	129	26	protons	proton	NOUN
eurjchem-289	129	27	)	)	PUNCT
eurjchem-289	129	28	,	,	PUNCT
eurjchem-289	129	29	9.05	9.05	NUM
eurjchem-289	129	30	,	,	PUNCT
eurjchem-289	129	31	9.15	9.15	NUM
eurjchem-289	129	32	and	and	CCONJ
eurjchem-289	129	33	10.95	10.95	NUM
eurjchem-289	129	34	(	(	PUNCT
eurjchem-289	129	35	s	s	PROPN
eurjchem-289	129	36	,	,	PUNCT
eurjchem-289	129	37	3h	3h	NUM
eurjchem-289	129	38	,	,	PUNCT
eurjchem-289	129	39	nh	nh	PROPN
eurjchem-289	129	40	exchanged	exchange	VERB
eurjchem-289	129	41	with	with	ADP
eurjchem-289	129	42	d2o	d2o	NOUN
eurjchem-289	129	43	)	)	PUNCT
eurjchem-289	129	44	.	.	PUNCT
eurjchem-289	130	1	anal	anal	PROPN
eurjchem-289	130	2	.	.	PUNCT
eurjchem-289	130	3	calcd	calcd	NOUN
eurjchem-289	130	4	.	.	PUNCT
eurjchem-289	131	1	for	for	ADP
eurjchem-289	131	2	c21h14n6o3	c21h14n6o3	PROPN
eurjchem-289	131	3	(	(	PUNCT
eurjchem-289	131	4	398	398	NUM
eurjchem-289	131	5	):	):	PUNCT
eurjchem-289	131	6	c	c	X
eurjchem-289	131	7	,	,	PUNCT
eurjchem-289	131	8	63.31	63.31	NUM
eurjchem-289	131	9	;	;	PUNCT
eurjchem-289	131	10	h	h	NOUN
eurjchem-289	131	11	,	,	PUNCT
eurjchem-289	131	12	3.51	3.51	NUM
eurjchem-289	131	13	;	;	PUNCT
eurjchem-289	131	14	n	n	CCONJ
eurjchem-289	131	15	,	,	PUNCT
eurjchem-289	131	16	21.10	21.10	NUM
eurjchem-289	131	17	.	.	PUNCT
eurjchem-289	131	18	found	find	VERB
eurjchem-289	131	19	:	:	PUNCT
eurjchem-289	132	1	c	c	X
eurjchem-289	132	2	,	,	PUNCT
eurjchem-289	132	3	63.57	63.57	NUM
eurjchem-289	132	4	;	;	PUNCT
eurjchem-289	132	5	h	h	X
eurjchem-289	132	6	,	,	PUNCT
eurjchem-289	132	7	3.84	3.84	NUM
eurjchem-289	132	8	;	;	PUNCT
eurjchem-289	132	9	n	n	CCONJ
eurjchem-289	132	10	,	,	PUNCT
eurjchem-289	132	11	20.86	20.86	NUM
eurjchem-289	132	12	%	%	NOUN
eurjchem-289	132	13	.	.	PUNCT
eurjchem-289	133	1	2.2.6	2.2.6	X
eurjchem-289	133	2	.	.	X
eurjchem-289	134	1	3‐(1‐methylidene‐2‐oxopropyl)quinoxalin‐2(1h)‐one	3‐(1‐methylidene‐2‐oxopropyl)quinoxalin‐2(1h)‐one	NUM
eurjchem-289	134	2	(	(	PUNCT
eurjchem-289	134	3	7	7	NUM
eurjchem-289	134	4	)	)	PUNCT
eurjchem-289	134	5	a	a	DET
eurjchem-289	134	6	solution	solution	NOUN
eurjchem-289	134	7	of	of	ADP
eurjchem-289	134	8	3‐acetonylquinoxalin‐2(1h)‐one	3‐acetonylquinoxalin‐2(1h)‐one	NUM
eurjchem-289	134	9	2	2	NUM
eurjchem-289	134	10	(	(	PUNCT
eurjchem-289	134	11	1.01	1.01	NUM
eurjchem-289	134	12	g	g	NOUN
eurjchem-289	134	13	,	,	PUNCT
eurjchem-289	134	14	0.005	0.005	NUM
eurjchem-289	134	15	mol	mol	NOUN
eurjchem-289	134	16	)	)	PUNCT
eurjchem-289	134	17	,	,	PUNCT
eurjchem-289	134	18	paraformaldehyde	paraformaldehyde	NOUN
eurjchem-289	134	19	(	(	PUNCT
eurjchem-289	134	20	0.15	0.15	NUM
eurjchem-289	134	21	g	g	NOUN
eurjchem-289	134	22	,	,	PUNCT
eurjchem-289	134	23	0.005	0.005	NUM
eurjchem-289	134	24	mol	mol	NOUN
eurjchem-289	134	25	)	)	PUNCT
eurjchem-289	134	26	in	in	ADP
eurjchem-289	134	27	acetic	acetic	ADJ
eurjchem-289	134	28	acid	acid	NOUN
eurjchem-289	134	29	(	(	PUNCT
eurjchem-289	134	30	1	1	NUM
eurjchem-289	134	31	ml	ml	NOUN
eurjchem-289	134	32	)	)	PUNCT
eurjchem-289	134	33	and	and	CCONJ
eurjchem-289	134	34	ethanol	ethanol	NOUN
eurjchem-289	134	35	(	(	PUNCT
eurjchem-289	134	36	10	10	NUM
eurjchem-289	134	37	ml	ml	NOUN
eurjchem-289	134	38	)	)	PUNCT
eurjchem-289	134	39	was	be	AUX
eurjchem-289	134	40	heated	heat	VERB
eurjchem-289	134	41	under	under	ADP
eurjchem-289	134	42	reflux	reflux	NOUN
eurjchem-289	134	43	for	for	ADP
eurjchem-289	134	44	3	3	NUM
eurjchem-289	134	45	h	h	NOUN
eurjchem-289	134	46	,	,	PUNCT
eurjchem-289	134	47	cooled	cool	VERB
eurjchem-289	134	48	and	and	CCONJ
eurjchem-289	134	49	the	the	DET
eurjchem-289	134	50	separated	separate	VERB
eurjchem-289	134	51	solid	solid	ADJ
eurjchem-289	134	52	was	be	AUX
eurjchem-289	134	53	filtered	filter	VERB
eurjchem-289	134	54	and	and	CCONJ
eurjchem-289	134	55	crystallized	crystallize	VERB
eurjchem-289	134	56	from	from	ADP
eurjchem-289	134	57	acetic	acetic	ADJ
eurjchem-289	134	58	acid	acid	NOUN
eurjchem-289	134	59	(	(	PUNCT
eurjchem-289	134	60	scheme	scheme	NOUN
eurjchem-289	134	61	1	1	NUM
eurjchem-289	134	62	)	)	PUNCT
eurjchem-289	134	63	.	.	PUNCT
eurjchem-289	135	1	yield	yield	NOUN
eurjchem-289	135	2	:	:	PUNCT
eurjchem-289	135	3	85	85	NUM
eurjchem-289	135	4	%	%	NOUN
eurjchem-289	135	5	.	.	PUNCT
eurjchem-289	136	1	m.p	m.p	PROPN
eurjchem-289	136	2	.	.	PROPN
eurjchem-289	136	3	:	:	PUNCT
eurjchem-289	137	1	277‐278	277‐278	ADJ
eurjchem-289	137	2	οc	οc	ADP
eurjchem-289	137	3	.	.	PROPN
eurjchem-289	137	4	ir	ir	PROPN
eurjchem-289	137	5	(	(	PUNCT
eurjchem-289	137	6	kbr	kbr	PROPN
eurjchem-289	137	7	,	,	PUNCT
eurjchem-289	137	8	cm‐1	cm‐1	PROPN
eurjchem-289	137	9	):	):	PUNCT
eurjchem-289	137	10	3400	3400	NUM
eurjchem-289	137	11	(	(	PUNCT
eurjchem-289	137	12	nh	nh	NOUN
eurjchem-289	137	13	)	)	PUNCT
eurjchem-289	137	14	,	,	PUNCT
eurjchem-289	137	15	1660	1660	NUM
eurjchem-289	137	16	,	,	PUNCT
eurjchem-289	137	17	1620	1620	NUM
eurjchem-289	137	18	(	(	PUNCT
eurjchem-289	137	19	c	c	NOUN
eurjchem-289	137	20	=	=	NOUN
eurjchem-289	137	21	o	o	NOUN
eurjchem-289	137	22	)	)	PUNCT
eurjchem-289	137	23	,	,	PUNCT
eurjchem-289	137	24	1375	1375	NUM
eurjchem-289	137	25	(	(	PUNCT
eurjchem-289	137	26	ch3	ch3	PROPN
eurjchem-289	137	27	bending	bending	NOUN
eurjchem-289	137	28	)	)	PUNCT
eurjchem-289	137	29	.	.	PUNCT
eurjchem-289	138	1	1h	1h	NUM
eurjchem-289	138	2	nmr	nmr	NOUN
eurjchem-289	138	3	(	(	PUNCT
eurjchem-289	138	4	chcl3	chcl3	PROPN
eurjchem-289	138	5	/	/	SYM
eurjchem-289	138	6	tfa	tfa	PROPN
eurjchem-289	138	7	,	,	PUNCT
eurjchem-289	138	8	(	(	PUNCT
eurjchem-289	138	9	5:1	5:1	NUM
eurjchem-289	138	10	)	)	PUNCT
eurjchem-289	138	11	,	,	PUNCT
eurjchem-289	138	12	δ	δ	PROPN
eurjchem-289	138	13	,	,	PUNCT
eurjchem-289	138	14	ppm	ppm	NUM
eurjchem-289	138	15	):	):	PUNCT
eurjchem-289	138	16	2.24	2.24	NUM
eurjchem-289	138	17	(	(	PUNCT
eurjchem-289	138	18	s	s	PROPN
eurjchem-289	138	19	,	,	PUNCT
eurjchem-289	138	20	3h	3h	NUM
eurjchem-289	138	21	,	,	PUNCT
eurjchem-289	138	22	ch3	ch3	PROPN
eurjchem-289	138	23	)	)	PUNCT
eurjchem-289	138	24	,	,	PUNCT
eurjchem-289	138	25	4.98	4.98	NUM
eurjchem-289	138	26	,	,	PUNCT
eurjchem-289	138	27	5.28	5.28	NUM
eurjchem-289	138	28	(	(	PUNCT
eurjchem-289	138	29	2s	2s	NUM
eurjchem-289	138	30	,	,	PUNCT
eurjchem-289	138	31	2h	2h	NUM
eurjchem-289	138	32	,	,	PUNCT
eurjchem-289	138	33	ch2	ch2	PROPN
eurjchem-289	138	34	)	)	PUNCT
eurjchem-289	138	35	,	,	PUNCT
eurjchem-289	138	36	7.50‐7.97	7.50‐7.97	NOUN
eurjchem-289	138	37	(	(	PUNCT
eurjchem-289	138	38	m	m	PROPN
eurjchem-289	138	39	,	,	PUNCT
eurjchem-289	138	40	4h	4h	NUM
eurjchem-289	138	41	,	,	PUNCT
eurjchem-289	138	42	aromatic	aromatic	ADJ
eurjchem-289	138	43	protons	proton	NOUN
eurjchem-289	138	44	)	)	PUNCT
eurjchem-289	138	45	.	.	PUNCT
eurjchem-289	139	1	ms	ms	NOUN
eurjchem-289	139	2	(	(	PUNCT
eurjchem-289	139	3	m	m	PROPN
eurjchem-289	139	4	/	/	SYM
eurjchem-289	139	5	z	z	NOUN
eurjchem-289	139	6	(	(	PUNCT
eurjchem-289	139	7	%	%	NOUN
eurjchem-289	139	8	)	)	PUNCT
eurjchem-289	139	9	):	):	PUNCT
eurjchem-289	139	10	53	53	NUM
eurjchem-289	139	11	(	(	PUNCT
eurjchem-289	139	12	100	100	NUM
eurjchem-289	139	13	%	%	NOUN
eurjchem-289	139	14	)	)	PUNCT
eurjchem-289	139	15	,	,	PUNCT
eurjchem-289	139	16	214	214	NUM
eurjchem-289	139	17	(	(	PUNCT
eurjchem-289	139	18	m+	m+	NOUN
eurjchem-289	139	19	.	.	PROPN
eurjchem-289	139	20	,	,	PUNCT
eurjchem-289	139	21	18	18	NUM
eurjchem-289	139	22	%	%	NOUN
eurjchem-289	139	23	)	)	PUNCT
eurjchem-289	139	24	.	.	PUNCT
eurjchem-289	140	1	anal	anal	PROPN
eurjchem-289	140	2	.	.	PUNCT
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eurjchem-289	140	4	.	.	PUNCT
eurjchem-289	141	1	for	for	ADP
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eurjchem-289	141	3	(	(	PUNCT
eurjchem-289	141	4	214	214	NUM
eurjchem-289	141	5	):	):	PUNCT
eurjchem-289	141	6	c	c	NOUN
eurjchem-289	141	7	,	,	PUNCT
eurjchem-289	141	8	67.28	67.28	NUM
eurjchem-289	141	9	;	;	PUNCT
eurjchem-289	141	10	h	h	X
eurjchem-289	141	11	,	,	PUNCT
eurjchem-289	141	12	4.67	4.67	NUM
eurjchem-289	141	13	;	;	PUNCT
eurjchem-289	141	14	n	n	CCONJ
eurjchem-289	141	15	,	,	PUNCT
eurjchem-289	141	16	13.08	13.08	NUM
eurjchem-289	141	17	.	.	PUNCT
eurjchem-289	141	18	found	find	VERB
eurjchem-289	141	19	:	:	PUNCT
eurjchem-289	142	1	c	c	X
eurjchem-289	142	2	,	,	PUNCT
eurjchem-289	142	3	67.40	67.40	NUM
eurjchem-289	142	4	;	;	PUNCT
eurjchem-289	143	1	h	h	NOUN
eurjchem-289	143	2	,	,	PUNCT
eurjchem-289	143	3	4.90	4.90	NUM
eurjchem-289	143	4	;	;	PUNCT
eurjchem-289	143	5	n	n	CCONJ
eurjchem-289	143	6	,	,	PUNCT
eurjchem-289	143	7	13.06	13.06	NUM
eurjchem-289	143	8	%	%	NOUN
eurjchem-289	143	9	.	.	PUNCT
eurjchem-289	144	1	2.2.7	2.2.7	X
eurjchem-289	144	2	.	.	PUNCT
eurjchem-289	145	1	3‐[2‐oxo‐1‐(piperidin‐1‐ylmethyl)propyl]quinoxalin‐	3‐[2‐oxo‐1‐(piperidin‐1‐ylmethyl)propyl]quinoxalin‐	NUM
eurjchem-289	145	2	2(1h)‐one	2(1h)‐one	NUM
eurjchem-289	145	3	(	(	PUNCT
eurjchem-289	145	4	8)	8)	NUM
eurjchem-289	145	5	a	a	DET
eurjchem-289	145	6	solution	solution	NOUN
eurjchem-289	145	7	of	of	ADP
eurjchem-289	145	8	2	2	NUM
eurjchem-289	145	9	(	(	PUNCT
eurjchem-289	145	10	1.01	1.01	NUM
eurjchem-289	145	11	g	g	NOUN
eurjchem-289	145	12	,	,	PUNCT
eurjchem-289	145	13	0.005	0.005	NUM
eurjchem-289	145	14	mol	mol	NOUN
eurjchem-289	145	15	)	)	PUNCT
eurjchem-289	145	16	,	,	PUNCT
eurjchem-289	145	17	paraformaldehyde	paraformaldehyde	NOUN
eurjchem-289	145	18	(	(	PUNCT
eurjchem-289	145	19	0.15	0.15	NUM
eurjchem-289	145	20	g	g	NOUN
eurjchem-289	145	21	,	,	PUNCT
eurjchem-289	145	22	0.005	0.005	NUM
eurjchem-289	145	23	mol	mol	NOUN
eurjchem-289	145	24	)	)	PUNCT
eurjchem-289	145	25	and	and	CCONJ
eurjchem-289	145	26	piperidine	piperidine	NOUN
eurjchem-289	145	27	(	(	PUNCT
eurjchem-289	145	28	0.005	0.005	NUM
eurjchem-289	145	29	mol	mol	NOUN
eurjchem-289	145	30	)	)	PUNCT
eurjchem-289	145	31	in	in	ADP
eurjchem-289	145	32	acetic	acetic	ADJ
eurjchem-289	145	33	acid	acid	NOUN
eurjchem-289	145	34	(	(	PUNCT
eurjchem-289	145	35	1	1	NUM
eurjchem-289	145	36	ml	ml	NOUN
eurjchem-289	145	37	)	)	PUNCT
eurjchem-289	145	38	and	and	CCONJ
eurjchem-289	145	39	ethanol	ethanol	NOUN
eurjchem-289	145	40	(	(	PUNCT
eurjchem-289	145	41	10	10	NUM
eurjchem-289	145	42	ml	ml	NOUN
eurjchem-289	145	43	)	)	PUNCT
eurjchem-289	145	44	was	be	AUX
eurjchem-289	145	45	heated	heat	VERB
eurjchem-289	145	46	under	under	ADP
eurjchem-289	145	47	reflux	reflux	NOUN
eurjchem-289	145	48	for	for	ADP
eurjchem-289	145	49	3	3	NUM
eurjchem-289	145	50	h	h	NOUN
eurjchem-289	145	51	,	,	PUNCT
eurjchem-289	145	52	cooled	cool	VERB
eurjchem-289	145	53	and	and	CCONJ
eurjchem-289	145	54	the	the	DET
eurjchem-289	145	55	separated	separate	VERB
eurjchem-289	145	56	solid	solid	ADJ
eurjchem-289	145	57	was	be	AUX
eurjchem-289	145	58	filtered	filter	VERB
eurjchem-289	145	59	and	and	CCONJ
eurjchem-289	145	60	crystallized	crystallize	VERB
eurjchem-289	145	61	from	from	ADP
eurjchem-289	145	62	acetic	acetic	ADJ
eurjchem-289	145	63	acid	acid	NOUN
eurjchem-289	145	64	(	(	PUNCT
eurjchem-289	145	65	scheme	scheme	NOUN
eurjchem-289	145	66	1	1	NUM
eurjchem-289	145	67	)	)	PUNCT
eurjchem-289	145	68	.	.	PUNCT
eurjchem-289	146	1	yield	yield	NOUN
eurjchem-289	146	2	:	:	PUNCT
eurjchem-289	146	3	75	75	NUM
eurjchem-289	146	4	%	%	NOUN
eurjchem-289	146	5	.	.	PUNCT
eurjchem-289	147	1	m.p	m.p	PROPN
eurjchem-289	147	2	.	.	PROPN
eurjchem-289	147	3	:	:	PUNCT
eurjchem-289	148	1	>	>	PUNCT
eurjchem-289	148	2	300	300	NUM
eurjchem-289	148	3	οc	οc	NOUN
eurjchem-289	148	4	.	.	PROPN
eurjchem-289	148	5	ir	ir	PROPN
eurjchem-289	148	6	(	(	PUNCT
eurjchem-289	148	7	kbr	kbr	PROPN
eurjchem-289	148	8	,	,	PUNCT
eurjchem-289	148	9	cm‐1	cm‐1	PROPN
eurjchem-289	148	10	):	):	PUNCT
eurjchem-289	148	11	3400	3400	NUM
eurjchem-289	148	12	(	(	PUNCT
eurjchem-289	148	13	nh	nh	NOUN
eurjchem-289	148	14	)	)	PUNCT
eurjchem-289	148	15	,	,	PUNCT
eurjchem-289	148	16	1680	1680	NUM
eurjchem-289	148	17	,	,	PUNCT
eurjchem-289	148	18	1650	1650	NUM
eurjchem-289	148	19	(	(	PUNCT
eurjchem-289	148	20	c	c	NOUN
eurjchem-289	148	21	=	=	NOUN
eurjchem-289	148	22	o	o	NOUN
eurjchem-289	148	23	)	)	PUNCT
eurjchem-289	148	24	,	,	PUNCT
eurjchem-289	148	25	1380	1380	NUM
eurjchem-289	148	26	(	(	PUNCT
eurjchem-289	148	27	ch3	ch3	PROPN
eurjchem-289	148	28	bending	bending	NOUN
eurjchem-289	148	29	)	)	PUNCT
eurjchem-289	148	30	.	.	PUNCT
eurjchem-289	149	1	1h	1h	NUM
eurjchem-289	149	2	nmr	nmr	NOUN
eurjchem-289	149	3	(	(	PUNCT
eurjchem-289	149	4	chcl3	chcl3	PROPN
eurjchem-289	149	5	/	/	SYM
eurjchem-289	149	6	tfa	tfa	PROPN
eurjchem-289	149	7	,	,	PUNCT
eurjchem-289	149	8	(	(	PUNCT
eurjchem-289	149	9	5:1	5:1	NUM
eurjchem-289	149	10	)	)	PUNCT
eurjchem-289	149	11	,	,	PUNCT
eurjchem-289	149	12	δ	δ	PROPN
eurjchem-289	149	13	,	,	PUNCT
eurjchem-289	149	14	ppm	ppm	NOUN
eurjchem-289	149	15	):	):	PUNCT
eurjchem-289	149	16	1.59‐1.94	1.59‐1.94	PROPN
eurjchem-289	149	17	(	(	PUNCT
eurjchem-289	149	18	br	br	PROPN
eurjchem-289	149	19	.	.	PROPN
eurjchem-289	149	20	,	,	PUNCT
eurjchem-289	149	21	6h	6h	NOUN
eurjchem-289	149	22	,	,	PUNCT
eurjchem-289	149	23	piperidine	piperidine	NOUN
eurjchem-289	149	24	)	)	PUNCT
eurjchem-289	149	25	,	,	PUNCT
eurjchem-289	149	26	2.38	2.38	NUM
eurjchem-289	149	27	(	(	PUNCT
eurjchem-289	149	28	s	s	PROPN
eurjchem-289	149	29	,	,	PUNCT
eurjchem-289	149	30	3h	3h	NUM
eurjchem-289	149	31	,	,	PUNCT
eurjchem-289	149	32	ch3	ch3	PROPN
eurjchem-289	149	33	)	)	PUNCT
eurjchem-289	149	34	,	,	PUNCT
eurjchem-289	149	35	3.03	3.03	NUM
eurjchem-289	149	36	(	(	PUNCT
eurjchem-289	149	37	br	br	PROPN
eurjchem-289	149	38	.	.	PROPN
eurjchem-289	149	39	,	,	PUNCT
eurjchem-289	149	40	4h	4h	NOUN
eurjchem-289	149	41	,	,	PUNCT
eurjchem-289	149	42	piperidine	piperidine	NOUN
eurjchem-289	149	43	)	)	PUNCT
eurjchem-289	149	44	,	,	PUNCT
eurjchem-289	149	45	3.37	3.37	NUM
eurjchem-289	149	46	(	(	PUNCT
eurjchem-289	149	47	s	s	PROPN
eurjchem-289	149	48	,	,	PUNCT
eurjchem-289	149	49	1h	1h	NUM
eurjchem-289	149	50	,	,	PUNCT
eurjchem-289	149	51	ch‐ch2	ch‐ch2	PROPN
eurjchem-289	149	52	)	)	PUNCT
eurjchem-289	149	53	,	,	PUNCT
eurjchem-289	149	54	3.90	3.90	NUM
eurjchem-289	149	55	(	(	PUNCT
eurjchem-289	149	56	d	d	NOUN
eurjchem-289	149	57	,	,	PUNCT
eurjchem-289	149	58	2h	2h	NUM
eurjchem-289	149	59	,	,	PUNCT
eurjchem-289	149	60	ch2n	ch2n	PROPN
eurjchem-289	149	61	)	)	PUNCT
eurjchem-289	149	62	,	,	PUNCT
eurjchem-289	149	63	7.47‐8.06	7.47‐8.06	NUM
eurjchem-289	149	64	(	(	PUNCT
eurjchem-289	149	65	m	m	PROPN
eurjchem-289	149	66	,	,	PUNCT
eurjchem-289	149	67	4h	4h	NUM
eurjchem-289	149	68	,	,	PUNCT
eurjchem-289	149	69	aromatic	aromatic	ADJ
eurjchem-289	149	70	protons	proton	NOUN
eurjchem-289	149	71	)	)	PUNCT
eurjchem-289	149	72	.	.	PUNCT
eurjchem-289	150	1	ms	ms	NOUN
eurjchem-289	150	2	(	(	PUNCT
eurjchem-289	150	3	m	m	PROPN
eurjchem-289	150	4	/	/	SYM
eurjchem-289	150	5	z	z	NOUN
eurjchem-289	150	6	(	(	PUNCT
eurjchem-289	150	7	%	%	NOUN
eurjchem-289	150	8	)	)	PUNCT
eurjchem-289	150	9	):	):	PUNCT
eurjchem-289	150	10	52	52	NUM
eurjchem-289	150	11	(	(	PUNCT
eurjchem-289	150	12	100	100	NUM
eurjchem-289	150	13	%	%	NOUN
eurjchem-289	150	14	)	)	PUNCT
eurjchem-289	150	15	,	,	PUNCT
eurjchem-289	150	16	300	300	NUM
eurjchem-289	150	17	(	(	PUNCT
eurjchem-289	150	18	m+1	m+1	X
eurjchem-289	150	19	┐	┐	NUM
eurjchem-289	150	20	+	+	NOUN
eurjchem-289	150	21	.	.	PROPN
eurjchem-289	150	22	,	,	PUNCT
eurjchem-289	150	23	28.5	28.5	NUM
eurjchem-289	150	24	%	%	NOUN
eurjchem-289	150	25	)	)	PUNCT
eurjchem-289	150	26	.	.	PUNCT
eurjchem-289	151	1	anal	anal	PROPN
eurjchem-289	151	2	.	.	PUNCT
eurjchem-289	151	3	calcd	calcd	NOUN
eurjchem-289	151	4	.	.	PUNCT
eurjchem-289	152	1	for	for	ADP
eurjchem-289	152	2	c17h21n3o2	c17h21n3o2	PROPN
eurjchem-289	152	3	(	(	PUNCT
eurjchem-289	152	4	299	299	NUM
eurjchem-289	152	5	):	):	PUNCT
eurjchem-289	152	6	c	c	X
eurjchem-289	152	7	,	,	PUNCT
eurjchem-289	152	8	68.22	68.22	NUM
eurjchem-289	152	9	;	;	PUNCT
eurjchem-289	152	10	h	h	X
eurjchem-289	152	11	,	,	PUNCT
eurjchem-289	152	12	7.02	7.02	NUM
eurjchem-289	152	13	;	;	PUNCT
eurjchem-289	152	14	n	n	CCONJ
eurjchem-289	152	15	,	,	PUNCT
eurjchem-289	152	16	14.04	14.04	NUM
eurjchem-289	152	17	.	.	PUNCT
eurjchem-289	152	18	found	find	VERB
eurjchem-289	152	19	:	:	PUNCT
eurjchem-289	153	1	c	c	X
eurjchem-289	153	2	,	,	PUNCT
eurjchem-289	153	3	68.58	68.58	NUM
eurjchem-289	153	4	;	;	PUNCT
eurjchem-289	153	5	h	h	NOUN
eurjchem-289	153	6	,	,	PUNCT
eurjchem-289	153	7	7.34	7.34	NUM
eurjchem-289	153	8	;	;	PUNCT
eurjchem-289	153	9	n	n	CCONJ
eurjchem-289	153	10	,	,	PUNCT
eurjchem-289	153	11	14.18	14.18	NUM
eurjchem-289	153	12	%	%	NOUN
eurjchem-289	153	13	.	.	PUNCT
eurjchem-289	154	1	2.2.8	2.2.8	NUM
eurjchem-289	154	2	.	.	PUNCT
eurjchem-289	154	3	2‐(2‐arylethenyl)furo[2,3‐b]quinoxalines	2‐(2‐arylethenyl)furo[2,3‐b]quinoxaline	NOUN
eurjchem-289	154	4	(	(	PUNCT
eurjchem-289	154	5	9a	9a	NOUN
eurjchem-289	154	6	,	,	PUNCT
eurjchem-289	154	7	b	b	NOUN
eurjchem-289	154	8	)	)	PUNCT
eurjchem-289	154	9	a	a	DET
eurjchem-289	154	10	mixture	mixture	NOUN
eurjchem-289	154	11	of	of	ADP
eurjchem-289	154	12	3a	3a	NUM
eurjchem-289	154	13	,	,	PUNCT
eurjchem-289	154	14	b	b	PROPN
eurjchem-289	154	15	(	(	PUNCT
eurjchem-289	154	16	0.003	0.003	NUM
eurjchem-289	154	17	mol	mol	NOUN
eurjchem-289	154	18	)	)	PUNCT
eurjchem-289	154	19	,	,	PUNCT
eurjchem-289	154	20	acetic	acetic	ADJ
eurjchem-289	154	21	anhydride	anhydride	NOUN
eurjchem-289	154	22	(	(	PUNCT
eurjchem-289	154	23	10	10	NUM
eurjchem-289	154	24	ml	ml	NOUN
eurjchem-289	154	25	)	)	PUNCT
eurjchem-289	154	26	and	and	CCONJ
eurjchem-289	154	27	sulphuric	sulphuric	PROPN
eurjchem-289	154	28	acid	acid	NOUN
eurjchem-289	154	29	(	(	PUNCT
eurjchem-289	154	30	few	few	ADJ
eurjchem-289	154	31	drops	drop	NOUN
eurjchem-289	154	32	)	)	PUNCT
eurjchem-289	154	33	was	be	AUX
eurjchem-289	154	34	heated	heat	VERB
eurjchem-289	154	35	under	under	ADP
eurjchem-289	154	36	reflux	reflux	NOUN
eurjchem-289	154	37	for	for	ADP
eurjchem-289	154	38	5	5	NUM
eurjchem-289	154	39	h.	h.	NOUN
eurjchem-289	154	40	the	the	DET
eurjchem-289	154	41	reaction	reaction	NOUN
eurjchem-289	154	42	mixture	mixture	NOUN
eurjchem-289	154	43	was	be	AUX
eurjchem-289	154	44	cooled	cool	VERB
eurjchem-289	154	45	and	and	CCONJ
eurjchem-289	154	46	poured	pour	VERB
eurjchem-289	154	47	on	on	ADP
eurjchem-289	154	48	ice	ice	NOUN
eurjchem-289	154	49	(	(	PUNCT
eurjchem-289	154	50	10	10	NUM
eurjchem-289	154	51	ml	ml	NOUN
eurjchem-289	154	52	)	)	PUNCT
eurjchem-289	154	53	and	and	CCONJ
eurjchem-289	154	54	stirred	stir	VERB
eurjchem-289	154	55	.	.	PUNCT
eurjchem-289	155	1	the	the	DET
eurjchem-289	155	2	formed	form	VERB
eurjchem-289	155	3	product	product	NOUN
eurjchem-289	155	4	was	be	AUX
eurjchem-289	155	5	filtered	filter	VERB
eurjchem-289	155	6	,	,	PUNCT
eurjchem-289	155	7	dried	dry	VERB
eurjchem-289	155	8	and	and	CCONJ
eurjchem-289	155	9	crystallized	crystallize	VERB
eurjchem-289	155	10	from	from	ADP
eurjchem-289	155	11	ethanol	ethanol	NOUN
eurjchem-289	155	12	(	(	PUNCT
eurjchem-289	155	13	scheme	scheme	NOUN
eurjchem-289	155	14	1	1	NUM
eurjchem-289	155	15	)	)	PUNCT
eurjchem-289	155	16	.	.	PUNCT
eurjchem-289	156	1	2‐(2‐phenylethenyl)furo[2,3‐b]quinoxalines	2‐(2‐phenylethenyl)furo[2,3‐b]quinoxalines	NUM
eurjchem-289	156	2	(	(	PUNCT
eurjchem-289	156	3	9a	9a	NOUN
eurjchem-289	156	4	):	):	PUNCT
eurjchem-289	156	5	yield	yield	NOUN
eurjchem-289	156	6	:	:	PUNCT
eurjchem-289	156	7	50	50	NUM
eurjchem-289	156	8	%	%	NOUN
eurjchem-289	156	9	.	.	PUNCT
eurjchem-289	157	1	m.p	m.p	PROPN
eurjchem-289	157	2	.	.	PROPN
eurjchem-289	157	3	:	:	PUNCT
eurjchem-289	158	1	>	>	PUNCT
eurjchem-289	158	2	300	300	NUM
eurjchem-289	158	3	οc	οc	NOUN
eurjchem-289	158	4	.	.	PROPN
eurjchem-289	158	5	ir	ir	PROPN
eurjchem-289	158	6	(	(	PUNCT
eurjchem-289	158	7	kbr	kbr	PROPN
eurjchem-289	158	8	,	,	PUNCT
eurjchem-289	158	9	cm‐1	cm‐1	PROPN
eurjchem-289	158	10	):	):	PUNCT
eurjchem-289	158	11	1660	1660	NUM
eurjchem-289	158	12	(	(	PUNCT
eurjchem-289	158	13	c	c	NOUN
eurjchem-289	158	14	=	=	SYM
eurjchem-289	158	15	n	n	NUM
eurjchem-289	158	16	)	)	PUNCT
eurjchem-289	158	17	.	.	PUNCT
eurjchem-289	159	1	ms	ms	NOUN
eurjchem-289	159	2	(	(	PUNCT
eurjchem-289	159	3	m	m	PROPN
eurjchem-289	159	4	/	/	SYM
eurjchem-289	159	5	z	z	NOUN
eurjchem-289	159	6	(	(	PUNCT
eurjchem-289	159	7	%	%	NOUN
eurjchem-289	159	8	)	)	PUNCT
eurjchem-289	159	9	):	):	PUNCT
eurjchem-289	159	10	69	69	NUM
eurjchem-289	159	11	(	(	PUNCT
eurjchem-289	159	12	100	100	NUM
eurjchem-289	159	13	%	%	NOUN
eurjchem-289	159	14	)	)	PUNCT
eurjchem-289	159	15	,	,	PUNCT
eurjchem-289	159	16	272	272	NUM
eurjchem-289	159	17	(	(	PUNCT
eurjchem-289	159	18	m+	m+	NUM
eurjchem-289	159	19	.	.	PROPN
eurjchem-289	159	20	,	,	PUNCT
eurjchem-289	159	21	26.69	26.69	NUM
eurjchem-289	159	22	%	%	NOUN
eurjchem-289	159	23	)	)	PUNCT
eurjchem-289	159	24	,	,	PUNCT
eurjchem-289	159	25	273	273	NUM
eurjchem-289	159	26	(	(	PUNCT
eurjchem-289	159	27	m+1	m+1	X
eurjchem-289	159	28	┐	┐	NUM
eurjchem-289	159	29	+	+	NOUN
eurjchem-289	159	30	.	.	PROPN
eurjchem-289	159	31	,	,	PUNCT
eurjchem-289	159	32	5.13	5.13	NUM
eurjchem-289	159	33	%	%	NOUN
eurjchem-289	159	34	)	)	PUNCT
eurjchem-289	159	35	.	.	PUNCT
eurjchem-289	160	1	anal	anal	PROPN
eurjchem-289	160	2	.	.	PUNCT
eurjchem-289	160	3	calcd	calcd	NOUN
eurjchem-289	160	4	.	.	PUNCT
eurjchem-289	161	1	for	for	ADP
eurjchem-289	161	2	c18h12n2o	c18h12n2o	NOUN
eurjchem-289	161	3	(	(	PUNCT
eurjchem-289	161	4	272	272	NUM
eurjchem-289	161	5	):	):	PUNCT
eurjchem-289	161	6	c	c	X
eurjchem-289	161	7	,	,	PUNCT
eurjchem-289	161	8	79.41	79.41	NUM
eurjchem-289	161	9	;	;	PUNCT
eurjchem-289	161	10	h	h	NOUN
eurjchem-289	161	11	,	,	PUNCT
eurjchem-289	161	12	4.41	4.41	NUM
eurjchem-289	161	13	;	;	PUNCT
eurjchem-289	161	14	n	n	CCONJ
eurjchem-289	161	15	,	,	PUNCT
eurjchem-289	161	16	10.29	10.29	NUM
eurjchem-289	161	17	.	.	PUNCT
eurjchem-289	161	18	found	find	VERB
eurjchem-289	161	19	:	:	PUNCT
eurjchem-289	162	1	c	c	X
eurjchem-289	162	2	,	,	PUNCT
eurjchem-289	162	3	79.34	79.34	NUM
eurjchem-289	162	4	;	;	PUNCT
eurjchem-289	162	5	h	h	NOUN
eurjchem-289	162	6	,	,	PUNCT
eurjchem-289	162	7	4.45	4.45	NUM
eurjchem-289	162	8	;	;	PUNCT
eurjchem-289	162	9	n	n	CCONJ
eurjchem-289	162	10	,	,	PUNCT
eurjchem-289	162	11	10.65	10.65	NUM
eurjchem-289	162	12	%	%	NOUN
eurjchem-289	162	13	.	.	PUNCT
eurjchem-289	163	1	2‐[2‐(4‐	2‐[2‐(4‐	NUM
eurjchem-289	163	2	chlorophenyl)ethenyl]furo[2,3‐b]quinoxalines	chlorophenyl)ethenyl]furo[2,3‐b]quinoxaline	NOUN
eurjchem-289	163	3	(	(	PUNCT
eurjchem-289	163	4	9b	9b	NUM
eurjchem-289	163	5	):	):	PUNCT
eurjchem-289	163	6	yield	yield	NOUN
eurjchem-289	163	7	:	:	PUNCT
eurjchem-289	163	8	55	55	NUM
eurjchem-289	163	9	%	%	NOUN
eurjchem-289	163	10	.	.	PUNCT
eurjchem-289	164	1	m.p	m.p	PROPN
eurjchem-289	164	2	.	.	PROPN
eurjchem-289	164	3	:	:	PUNCT
eurjchem-289	165	1	>	>	PUNCT
eurjchem-289	165	2	300	300	NUM
eurjchem-289	165	3	οc	οc	NOUN
eurjchem-289	165	4	.	.	PROPN
eurjchem-289	165	5	ir	ir	PROPN
eurjchem-289	165	6	(	(	PUNCT
eurjchem-289	165	7	kbr	kbr	PROPN
eurjchem-289	165	8	,	,	PUNCT
eurjchem-289	165	9	cm‐1	cm‐1	PROPN
eurjchem-289	165	10	):	):	PUNCT
eurjchem-289	165	11	1650(c	1650(c	NOUN
eurjchem-289	165	12	=	=	SYM
eurjchem-289	165	13	n	n	CCONJ
eurjchem-289	165	14	)	)	PUNCT
eurjchem-289	165	15	.	.	PUNCT
eurjchem-289	166	1	1h	1h	NUM
eurjchem-289	166	2	nmr	nmr	NOUN
eurjchem-289	166	3	(	(	PUNCT
eurjchem-289	166	4	dmso‐d6	dmso‐d6	PROPN
eurjchem-289	166	5	,	,	PUNCT
eurjchem-289	166	6	δ	δ	PROPN
eurjchem-289	166	7	,	,	PUNCT
eurjchem-289	166	8	ppm	ppm	NUM
eurjchem-289	166	9	):	):	PUNCT
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eurjchem-289	166	11	(	(	PUNCT
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eurjchem-289	166	18	)	)	PUNCT
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eurjchem-289	167	5	z	z	NOUN
eurjchem-289	167	6	(	(	PUNCT
eurjchem-289	167	7	%	%	NOUN
eurjchem-289	167	8	)	)	PUNCT
eurjchem-289	167	9	):	):	PUNCT
eurjchem-289	167	10	306	306	NUM
eurjchem-289	167	11	(	(	PUNCT
eurjchem-289	167	12	m+	m+	NOUN
eurjchem-289	167	13	.	.	PROPN
eurjchem-289	167	14	,	,	PUNCT
eurjchem-289	167	15	100	100	NUM
eurjchem-289	167	16	%	%	NOUN
eurjchem-289	167	17	)	)	PUNCT
eurjchem-289	167	18	,	,	PUNCT
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eurjchem-289	167	20	(	(	PUNCT
eurjchem-289	167	21	m+1	m+1	X
eurjchem-289	167	22	┐	┐	NUM
eurjchem-289	167	23	+	+	NOUN
eurjchem-289	167	24	.	.	PROPN
eurjchem-289	167	25	,	,	PUNCT
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eurjchem-289	167	27	%	%	NOUN
eurjchem-289	167	28	)	)	PUNCT
eurjchem-289	167	29	,	,	PUNCT
eurjchem-289	167	30	308(m+2	308(m+2	PROPN
eurjchem-289	167	31	┐	┐	PROPN
eurjchem-289	167	32	+	+	PROPN
eurjchem-289	167	33	.	.	PROPN
eurjchem-289	167	34	,	,	PUNCT
eurjchem-289	167	35	32.11	32.11	NUM
eurjchem-289	167	36	%	%	NOUN
eurjchem-289	167	37	)	)	PUNCT
eurjchem-289	167	38	.	.	PUNCT
eurjchem-289	168	1	anal	anal	PROPN
eurjchem-289	168	2	.	.	PUNCT
eurjchem-289	168	3	calcd	calcd	NOUN
eurjchem-289	168	4	.	.	PUNCT
eurjchem-289	169	1	for	for	SCONJ
eurjchem-289	169	2	c18h11cln2o	c18h11cln2o	NOUN
eurjchem-289	169	3	(	(	PUNCT
eurjchem-289	169	4	306.5	306.5	NUM
eurjchem-289	169	5	):	):	PUNCT
eurjchem-289	169	6	c	c	NOUN
eurjchem-289	169	7	,	,	PUNCT
eurjchem-289	169	8	70.47	70.47	NUM
eurjchem-289	169	9	;	;	PUNCT
eurjchem-289	169	10	h	h	NOUN
eurjchem-289	169	11	,	,	PUNCT
eurjchem-289	169	12	3.59	3.59	NUM
eurjchem-289	169	13	;	;	PUNCT
eurjchem-289	169	14	n	n	CCONJ
eurjchem-289	169	15	,	,	PUNCT
eurjchem-289	169	16	9.14	9.14	NUM
eurjchem-289	169	17	.	.	PUNCT
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eurjchem-289	169	19	:	:	PUNCT
eurjchem-289	170	1	c	c	X
eurjchem-289	170	2	,	,	PUNCT
eurjchem-289	170	3	70.72	70.72	NUM
eurjchem-289	170	4	;	;	PUNCT
eurjchem-289	170	5	h	h	NOUN
eurjchem-289	170	6	,	,	PUNCT
eurjchem-289	170	7	3.33	3.33	NUM
eurjchem-289	170	8	;	;	PUNCT
eurjchem-289	170	9	n	n	CCONJ
eurjchem-289	170	10	,	,	PUNCT
eurjchem-289	170	11	9.46	9.46	NUM
eurjchem-289	170	12	.	.	PUNCT
eurjchem-289	171	1	2.2.9	2.2.9	NUM
eurjchem-289	171	2	.	.	PUNCT
eurjchem-289	172	1	3‐[(5‐aryl‐1h‐pyrazol‐3‐yl)methyl]quinoxalin‐2(1h)‐	3‐[(5‐aryl‐1h‐pyrazol‐3‐yl)methyl]quinoxalin‐2(1h)‐	ADJ
eurjchem-289	172	2	ones	one	NOUN
eurjchem-289	172	3	(	(	PUNCT
eurjchem-289	172	4	10a	10a	NOUN
eurjchem-289	172	5	,	,	PUNCT
eurjchem-289	172	6	b	b	NOUN
eurjchem-289	172	7	)	)	PUNCT
eurjchem-289	172	8	a	a	DET
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eurjchem-289	172	10	of	of	ADP
eurjchem-289	172	11	3c	3c	NUM
eurjchem-289	172	12	,	,	PUNCT
eurjchem-289	172	13	d	d	X
eurjchem-289	172	14	(	(	PUNCT
eurjchem-289	172	15	0.003	0.003	NUM
eurjchem-289	172	16	mol	mol	NOUN
eurjchem-289	172	17	)	)	PUNCT
eurjchem-289	172	18	and	and	CCONJ
eurjchem-289	172	19	99	99	NUM
eurjchem-289	172	20	%	%	NOUN
eurjchem-289	172	21	hydrazine	hydrazine	NOUN
eurjchem-289	172	22	hydrate	hydrate	NOUN
eurjchem-289	172	23	(	(	PUNCT
eurjchem-289	172	24	0.75	0.75	NUM
eurjchem-289	172	25	g	g	NOUN
eurjchem-289	172	26	,	,	PUNCT
eurjchem-289	172	27	0.015	0.015	NUM
eurjchem-289	172	28	mol	mol	NOUN
eurjchem-289	172	29	)	)	PUNCT
eurjchem-289	172	30	in	in	ADP
eurjchem-289	172	31	absolute	absolute	ADJ
eurjchem-289	172	32	ethanol	ethanol	NOUN
eurjchem-289	172	33	(	(	PUNCT
eurjchem-289	172	34	15	15	NUM
eurjchem-289	172	35	ml	ml	NOUN
eurjchem-289	172	36	)	)	PUNCT
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eurjchem-289	172	38	few	few	ADJ
eurjchem-289	172	39	drops	drop	NOUN
eurjchem-289	172	40	of	of	ADP
eurjchem-289	172	41	glacial	glacial	ADJ
eurjchem-289	172	42	acetic	acetic	ADJ
eurjchem-289	172	43	acid	acid	NOUN
eurjchem-289	172	44	was	be	AUX
eurjchem-289	172	45	heated	heat	VERB
eurjchem-289	172	46	under	under	ADP
eurjchem-289	172	47	reflux	reflux	NOUN
eurjchem-289	172	48	for	for	ADP
eurjchem-289	172	49	5	5	NUM
eurjchem-289	172	50	h.	h.	NOUN
eurjchem-289	172	51	the	the	DET
eurjchem-289	172	52	reaction	reaction	NOUN
eurjchem-289	172	53	mixture	mixture	NOUN
eurjchem-289	172	54	was	be	AUX
eurjchem-289	172	55	cooled	cool	VERB
eurjchem-289	172	56	,	,	PUNCT
eurjchem-289	172	57	and	and	CCONJ
eurjchem-289	172	58	the	the	DET
eurjchem-289	172	59	formed	form	VERB
eurjchem-289	172	60	solid	solid	ADJ
eurjchem-289	172	61	was	be	AUX
eurjchem-289	172	62	filtered	filter	VERB
eurjchem-289	172	63	,	,	PUNCT
eurjchem-289	172	64	dried	dry	VERB
eurjchem-289	172	65	and	and	CCONJ
eurjchem-289	172	66	crystallized	crystallize	VERB
eurjchem-289	172	67	from	from	ADP
eurjchem-289	172	68	acetone	acetone	NOUN
eurjchem-289	172	69	(	(	PUNCT
eurjchem-289	172	70	scheme	scheme	NOUN
eurjchem-289	172	71	1	1	NUM
eurjchem-289	172	72	)	)	PUNCT
eurjchem-289	172	73	.	.	PUNCT
eurjchem-289	173	1	3‐{[5‐(3‐nitrophenyl)‐1h‐pyrazol‐3‐yl]methyl}quinoxalin‐	3‐{[5‐(3‐nitrophenyl)‐1h‐pyrazol‐3‐yl]methyl}quinoxalin‐	NUM
eurjchem-289	173	2	2(1h)‐ones	2(1h)‐ones	NUM
eurjchem-289	173	3	(	(	PUNCT
eurjchem-289	173	4	10a	10a	NUM
eurjchem-289	173	5	):	):	PUNCT
eurjchem-289	173	6	yield	yield	NOUN
eurjchem-289	173	7	:	:	PUNCT
eurjchem-289	173	8	50	50	NUM
eurjchem-289	173	9	%	%	NOUN
eurjchem-289	173	10	.	.	PUNCT
eurjchem-289	174	1	m.p	m.p	PROPN
eurjchem-289	174	2	.	.	PROPN
eurjchem-289	174	3	:	:	PUNCT
eurjchem-289	175	1	232‐234	232‐234	NUM
eurjchem-289	175	2	οc	οc	PROPN
eurjchem-289	175	3	.	.	PROPN
eurjchem-289	175	4	ir	ir	PROPN
eurjchem-289	175	5	(	(	PUNCT
eurjchem-289	175	6	kbr	kbr	PROPN
eurjchem-289	175	7	,	,	PUNCT
eurjchem-289	175	8	cm‐1	cm‐1	PROPN
eurjchem-289	175	9	):	):	PUNCT
eurjchem-289	175	10	3300‐3250	3300‐3250	NUM
eurjchem-289	175	11	(	(	PUNCT
eurjchem-289	175	12	nh	nh	NOUN
eurjchem-289	175	13	)	)	PUNCT
eurjchem-289	175	14	,	,	PUNCT
eurjchem-289	175	15	1685	1685	NUM
eurjchem-289	175	16	(	(	PUNCT
eurjchem-289	175	17	c	c	NOUN
eurjchem-289	175	18	=	=	NOUN
eurjchem-289	175	19	o	o	NOUN
eurjchem-289	175	20	)	)	PUNCT
eurjchem-289	175	21	.	.	PUNCT
eurjchem-289	176	1	368	368	NUM
eurjchem-289	176	2	shabaan	shabaan	VERB
eurjchem-289	176	3	et	et	PROPN
eurjchem-289	176	4	al	al	PROPN
eurjchem-289	176	5	.	.	PUNCT
eurjchem-289	176	6	/	/	SYM
eurjchem-289	176	7	european	european	PROPN
eurjchem-289	176	8	journal	journal	PROPN
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eurjchem-289	176	10	chemistry	chemistry	NOUN
eurjchem-289	176	11	2	2	NUM
eurjchem-289	176	12	(	(	PUNCT
eurjchem-289	176	13	3	3	NUM
eurjchem-289	176	14	)	)	PUNCT
eurjchem-289	176	15	(	(	PUNCT
eurjchem-289	176	16	2011	2011	NUM
eurjchem-289	176	17	)	)	PUNCT
eurjchem-289	176	18	365‐371	365‐371	NUM
eurjchem-289	176	19	scheme	scheme	NOUN
eurjchem-289	176	20	2	2	NUM
eurjchem-289	176	21	1h	1h	NUM
eurjchem-289	176	22	nmr	nmr	NOUN
eurjchem-289	176	23	(	(	PUNCT
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eurjchem-289	176	25	,	,	PUNCT
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eurjchem-289	176	27	,	,	PUNCT
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eurjchem-289	176	29	):	):	PUNCT
eurjchem-289	176	30	4.27	4.27	NUM
eurjchem-289	176	31	(	(	PUNCT
eurjchem-289	176	32	s	s	PROPN
eurjchem-289	176	33	,	,	PUNCT
eurjchem-289	176	34	2h	2h	NUM
eurjchem-289	176	35	,	,	PUNCT
eurjchem-289	176	36	ch2	ch2	PROPN
eurjchem-289	176	37	)	)	PUNCT
eurjchem-289	176	38	,	,	PUNCT
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eurjchem-289	176	40	(	(	PUNCT
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eurjchem-289	176	42	,	,	PUNCT
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eurjchem-289	176	44	,	,	PUNCT
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eurjchem-289	176	47	)	)	PUNCT
eurjchem-289	176	48	,	,	PUNCT
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eurjchem-289	176	50	,	,	PUNCT
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eurjchem-289	176	54	,	,	PUNCT
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eurjchem-289	176	63	.	.	PUNCT
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eurjchem-289	177	6	(	(	PUNCT
eurjchem-289	177	7	%	%	NOUN
eurjchem-289	177	8	)	)	PUNCT
eurjchem-289	177	9	):	):	PUNCT
eurjchem-289	177	10	347	347	NUM
eurjchem-289	177	11	(	(	PUNCT
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eurjchem-289	177	14	,	,	PUNCT
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eurjchem-289	177	16	%	%	NOUN
eurjchem-289	177	17	)	)	PUNCT
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eurjchem-289	177	25	,	,	PUNCT
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eurjchem-289	177	28	)	)	PUNCT
eurjchem-289	177	29	.	.	PUNCT
eurjchem-289	178	1	anal	anal	PROPN
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eurjchem-289	179	3	(	(	PUNCT
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eurjchem-289	179	5	):	):	PUNCT
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eurjchem-289	179	7	,	,	PUNCT
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eurjchem-289	180	1	c	c	X
eurjchem-289	180	2	,	,	PUNCT
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eurjchem-289	180	4	;	;	PUNCT
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eurjchem-289	181	4	;	;	PUNCT
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eurjchem-289	181	9	.	.	PUNCT
eurjchem-289	182	1	3‐{[5‐(4‐fluorophenyl)‐1h‐pyrazol‐3‐yl]methyl}quinoxalin‐	3‐{[5‐(4‐fluorophenyl)‐1h‐pyrazol‐3‐yl]methyl}quinoxalin‐	NUM
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eurjchem-289	182	5	):	):	PUNCT
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eurjchem-289	182	7	:	:	PUNCT
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eurjchem-289	182	10	.	.	PUNCT
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eurjchem-289	183	3	:	:	PUNCT
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eurjchem-289	184	7	,	,	PUNCT
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eurjchem-289	184	9	):	):	PUNCT
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eurjchem-289	184	11	(	(	PUNCT
eurjchem-289	184	12	nh	nh	NOUN
eurjchem-289	184	13	)	)	PUNCT
eurjchem-289	184	14	,	,	PUNCT
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eurjchem-289	184	16	(	(	PUNCT
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eurjchem-289	184	18	=	=	NOUN
eurjchem-289	184	19	o	o	NOUN
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eurjchem-289	184	21	.	.	PUNCT
eurjchem-289	185	1	1h	1h	NUM
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eurjchem-289	185	5	,	,	PUNCT
eurjchem-289	185	6	δ	δ	PROPN
eurjchem-289	185	7	,	,	PUNCT
eurjchem-289	185	8	ppm	ppm	NOUN
eurjchem-289	185	9	):	):	PUNCT
eurjchem-289	185	10	4.17	4.17	NUM
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eurjchem-289	185	13	,	,	PUNCT
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eurjchem-289	185	15	,	,	PUNCT
eurjchem-289	185	16	ch2	ch2	PROPN
eurjchem-289	185	17	)	)	PUNCT
eurjchem-289	185	18	,	,	PUNCT
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eurjchem-289	185	28	,	,	PUNCT
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eurjchem-289	185	30	,	,	PUNCT
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eurjchem-289	185	32	(	(	PUNCT
eurjchem-289	185	33	2s	2s	NUM
eurjchem-289	185	34	,	,	PUNCT
eurjchem-289	185	35	2h	2h	NUM
eurjchem-289	185	36	,	,	PUNCT
eurjchem-289	185	37	2nh	2nh	NOUN
eurjchem-289	185	38	,	,	PUNCT
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eurjchem-289	185	40	with	with	ADP
eurjchem-289	185	41	d2o	d2o	NOUN
eurjchem-289	185	42	)	)	PUNCT
eurjchem-289	185	43	.	.	PUNCT
eurjchem-289	186	1	anal	anal	PROPN
eurjchem-289	186	2	.	.	PUNCT
eurjchem-289	186	3	calcd	calcd	NOUN
eurjchem-289	186	4	.	.	PUNCT
eurjchem-289	187	1	for	for	SCONJ
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eurjchem-289	187	3	(	(	PUNCT
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eurjchem-289	187	5	):	):	PUNCT
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eurjchem-289	187	7	,	,	PUNCT
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eurjchem-289	187	9	;	;	PUNCT
eurjchem-289	187	10	h	h	NOUN
eurjchem-289	187	11	,	,	PUNCT
eurjchem-289	187	12	4.06	4.06	NUM
eurjchem-289	187	13	;	;	PUNCT
eurjchem-289	187	14	n	n	CCONJ
eurjchem-289	187	15	,	,	PUNCT
eurjchem-289	187	16	17.50	17.50	NUM
eurjchem-289	187	17	.	.	PUNCT
eurjchem-289	187	18	found	find	VERB
eurjchem-289	187	19	:	:	PUNCT
eurjchem-289	188	1	c	c	X
eurjchem-289	188	2	,	,	PUNCT
eurjchem-289	188	3	67.50	67.50	NUM
eurjchem-289	188	4	;	;	PUNCT
eurjchem-289	188	5	h	h	NOUN
eurjchem-289	188	6	,	,	PUNCT
eurjchem-289	188	7	4.11	4.11	NUM
eurjchem-289	188	8	;	;	PUNCT
eurjchem-289	188	9	n	n	CCONJ
eurjchem-289	188	10	,	,	PUNCT
eurjchem-289	188	11	17.37	17.37	NUM
eurjchem-289	188	12	%	%	NOUN
eurjchem-289	188	13	.	.	PUNCT
eurjchem-289	189	1	2.2.10	2.2.10	NUM
eurjchem-289	189	2	.	.	PUNCT
eurjchem-289	190	1	3‐[1‐(2‐arylhydrazinylidene)‐2‐oxopropyl	3‐[1‐(2‐arylhydrazinylidene)‐2‐oxopropyl	NUM
eurjchem-289	190	2	]	]	PUNCT
eurjchem-289	190	3	quinoxalin‐2(1h)‐ones	quinoxalin‐2(1h)‐one	NOUN
eurjchem-289	190	4	(	(	PUNCT
eurjchem-289	190	5	11a	11a	NOUN
eurjchem-289	190	6	,	,	PUNCT
eurjchem-289	190	7	b	b	X
eurjchem-289	190	8	)	)	PUNCT
eurjchem-289	190	9	a	a	DET
eurjchem-289	190	10	mixture	mixture	NOUN
eurjchem-289	190	11	of	of	ADP
eurjchem-289	190	12	2	2	NUM
eurjchem-289	190	13	(	(	PUNCT
eurjchem-289	190	14	2.02	2.02	NUM
eurjchem-289	190	15	g	g	NOUN
eurjchem-289	190	16	,	,	PUNCT
eurjchem-289	190	17	0.01	0.01	NUM
eurjchem-289	190	18	mol	mol	NOUN
eurjchem-289	190	19	)	)	PUNCT
eurjchem-289	190	20	,	,	PUNCT
eurjchem-289	190	21	sodium	sodium	NOUN
eurjchem-289	190	22	hydroxide	hydroxide	NOUN
eurjchem-289	190	23	(	(	PUNCT
eurjchem-289	190	24	1.6	1.6	NUM
eurjchem-289	190	25	g	g	NOUN
eurjchem-289	190	26	,	,	PUNCT
eurjchem-289	190	27	0.04	0.04	NUM
eurjchem-289	190	28	mol	mol	NOUN
eurjchem-289	190	29	)	)	PUNCT
eurjchem-289	190	30	and	and	CCONJ
eurjchem-289	190	31	water	water	NOUN
eurjchem-289	190	32	(	(	PUNCT
eurjchem-289	190	33	25	25	NUM
eurjchem-289	190	34	ml	ml	NOUN
eurjchem-289	190	35	)	)	PUNCT
eurjchem-289	190	36	was	be	AUX
eurjchem-289	190	37	stirred	stir	VERB
eurjchem-289	190	38	for	for	ADP
eurjchem-289	190	39	10	10	NUM
eurjchem-289	190	40	min	min	NOUN
eurjchem-289	190	41	until	until	SCONJ
eurjchem-289	190	42	a	a	DET
eurjchem-289	190	43	clear	clear	ADJ
eurjchem-289	190	44	solution	solution	NOUN
eurjchem-289	190	45	was	be	AUX
eurjchem-289	190	46	formed	form	VERB
eurjchem-289	190	47	,	,	PUNCT
eurjchem-289	190	48	then	then	ADV
eurjchem-289	190	49	chilled	chill	VERB
eurjchem-289	190	50	at	at	ADP
eurjchem-289	190	51	‐5	‐5	NUM
eurjchem-289	190	52	°	°	PROPN
eurjchem-289	190	53	c	c	NOUN
eurjchem-289	190	54	.	.	PUNCT
eurjchem-289	191	1	to	to	ADP
eurjchem-289	191	2	this	this	DET
eurjchem-289	191	3	solution	solution	NOUN
eurjchem-289	191	4	,	,	PUNCT
eurjchem-289	191	5	an	an	DET
eurjchem-289	191	6	ice	ice	NOUN
eurjchem-289	191	7	cooled	cool	VERB
eurjchem-289	191	8	solution	solution	NOUN
eurjchem-289	191	9	of	of	ADP
eurjchem-289	191	10	aryldiazonium	aryldiazonium	NOUN
eurjchem-289	191	11	salt	salt	NOUN
eurjchem-289	191	12	[	[	X
eurjchem-289	191	13	prepared	prepare	VERB
eurjchem-289	191	14	from	from	ADP
eurjchem-289	191	15	the	the	DET
eurjchem-289	191	16	appropriate	appropriate	ADJ
eurjchem-289	191	17	aromatic	aromatic	ADJ
eurjchem-289	191	18	amine	amine	NOUN
eurjchem-289	191	19	(	(	PUNCT
eurjchem-289	191	20	0.01	0.01	NUM
eurjchem-289	191	21	mol	mol	NOUN
eurjchem-289	191	22	)	)	PUNCT
eurjchem-289	191	23	,	,	PUNCT
eurjchem-289	191	24	concentrated	concentrated	ADJ
eurjchem-289	191	25	hydrochloric	hydrochloric	ADJ
eurjchem-289	191	26	acid	acid	NOUN
eurjchem-289	191	27	(	(	PUNCT
eurjchem-289	191	28	3	3	NUM
eurjchem-289	191	29	ml	ml	NOUN
eurjchem-289	191	30	)	)	PUNCT
eurjchem-289	191	31	and	and	CCONJ
eurjchem-289	191	32	sodium	sodium	NOUN
eurjchem-289	191	33	nitrite	nitrite	NOUN
eurjchem-289	191	34	(	(	PUNCT
eurjchem-289	191	35	0.69	0.69	NUM
eurjchem-289	191	36	g	g	NOUN
eurjchem-289	191	37	,	,	PUNCT
eurjchem-289	191	38	0.01	0.01	NUM
eurjchem-289	191	39	mol	mol	NOUN
eurjchem-289	191	40	)	)	PUNCT
eurjchem-289	191	41	in	in	ADP
eurjchem-289	191	42	water	water	NOUN
eurjchem-289	191	43	(	(	PUNCT
eurjchem-289	191	44	15	15	NUM
eurjchem-289	191	45	ml	ml	NOUN
eurjchem-289	191	46	)	)	PUNCT
eurjchem-289	191	47	]	]	PUNCT
eurjchem-289	191	48	was	be	AUX
eurjchem-289	191	49	added	add	VERB
eurjchem-289	191	50	.	.	PUNCT
eurjchem-289	192	1	the	the	DET
eurjchem-289	192	2	reaction	reaction	NOUN
eurjchem-289	192	3	mixture	mixture	NOUN
eurjchem-289	192	4	was	be	AUX
eurjchem-289	192	5	maintained	maintain	VERB
eurjchem-289	192	6	at	at	ADP
eurjchem-289	192	7	‐5	‐5	PROPN
eurjchem-289	192	8	°	°	ADP
eurjchem-289	192	9	c	c	PROPN
eurjchem-289	192	10	for	for	ADP
eurjchem-289	192	11	30	30	NUM
eurjchem-289	192	12	min	min	NOUN
eurjchem-289	192	13	then	then	ADV
eurjchem-289	192	14	acidified	acidify	VERB
eurjchem-289	192	15	with	with	ADP
eurjchem-289	192	16	glacial	glacial	ADJ
eurjchem-289	192	17	acetic	acetic	ADJ
eurjchem-289	192	18	acid	acid	NOUN
eurjchem-289	192	19	till	till	SCONJ
eurjchem-289	192	20	ph	ph	NOUN
eurjchem-289	192	21	5‐5.5	5‐5.5	PROPN
eurjchem-289	192	22	.	.	PUNCT
eurjchem-289	193	1	the	the	DET
eurjchem-289	193	2	formed	form	VERB
eurjchem-289	193	3	solid	solid	ADJ
eurjchem-289	193	4	was	be	AUX
eurjchem-289	193	5	filtered	filter	VERB
eurjchem-289	193	6	,	,	PUNCT
eurjchem-289	193	7	washed	wash	VERB
eurjchem-289	193	8	with	with	ADP
eurjchem-289	193	9	water	water	NOUN
eurjchem-289	193	10	and	and	CCONJ
eurjchem-289	193	11	crystallized	crystallize	VERB
eurjchem-289	193	12	from	from	ADP
eurjchem-289	193	13	ethyl	ethyl	PROPN
eurjchem-289	193	14	acetate	acetate	PROPN
eurjchem-289	193	15	(	(	PUNCT
eurjchem-289	193	16	scheme	scheme	NOUN
eurjchem-289	193	17	2	2	NUM
eurjchem-289	193	18	)	)	PUNCT
eurjchem-289	193	19	.	.	PUNCT
eurjchem-289	194	1	3‐[1‐(2‐phenylhydrazinylidene)‐2‐oxopropyl]quinoxalin‐	3‐[1‐(2‐phenylhydrazinylidene)‐2‐oxopropyl]quinoxalin‐	ADJ
eurjchem-289	194	2	2(1h)‐ones	2(1h)‐ones	NUM
eurjchem-289	194	3	(	(	PUNCT
eurjchem-289	194	4	11a	11a	NUM
eurjchem-289	194	5	):	):	PUNCT
eurjchem-289	194	6	yield	yield	NOUN
eurjchem-289	194	7	:	:	PUNCT
eurjchem-289	194	8	60	60	NUM
eurjchem-289	194	9	%	%	NOUN
eurjchem-289	194	10	.	.	PUNCT
eurjchem-289	195	1	m.p	m.p	PROPN
eurjchem-289	195	2	.	.	PROPN
eurjchem-289	195	3	:	:	PUNCT
eurjchem-289	196	1	140‐142	140‐142	NUM
eurjchem-289	196	2	οc	οc	ADP
eurjchem-289	196	3	.	.	PROPN
eurjchem-289	196	4	ir	ir	PROPN
eurjchem-289	196	5	(	(	PUNCT
eurjchem-289	196	6	kbr	kbr	PROPN
eurjchem-289	196	7	,	,	PUNCT
eurjchem-289	196	8	cm‐1	cm‐1	PROPN
eurjchem-289	196	9	):	):	PUNCT
eurjchem-289	196	10	3500‐3450	3500‐3450	NUM
eurjchem-289	196	11	(	(	PUNCT
eurjchem-289	196	12	nh	nh	NOUN
eurjchem-289	196	13	)	)	PUNCT
eurjchem-289	196	14	,	,	PUNCT
eurjchem-289	196	15	1690	1690	NUM
eurjchem-289	196	16	,	,	PUNCT
eurjchem-289	196	17	1675	1675	NUM
eurjchem-289	196	18	(	(	PUNCT
eurjchem-289	196	19	c	c	NOUN
eurjchem-289	196	20	=	=	NOUN
eurjchem-289	196	21	o	o	NOUN
eurjchem-289	196	22	)	)	PUNCT
eurjchem-289	196	23	,	,	PUNCT
eurjchem-289	196	24	1370	1370	NUM
eurjchem-289	196	25	(	(	PUNCT
eurjchem-289	196	26	ch3	ch3	PROPN
eurjchem-289	196	27	bending	bending	NOUN
eurjchem-289	196	28	)	)	PUNCT
eurjchem-289	196	29	.	.	PUNCT
eurjchem-289	197	1	1h	1h	NUM
eurjchem-289	197	2	nmr	nmr	NOUN
eurjchem-289	197	3	(	(	PUNCT
eurjchem-289	197	4	dmso‐d6	dmso‐d6	PROPN
eurjchem-289	197	5	,	,	PUNCT
eurjchem-289	197	6	δ	δ	PROPN
eurjchem-289	197	7	,	,	PUNCT
eurjchem-289	197	8	ppm	ppm	NUM
eurjchem-289	197	9	):	):	PUNCT
eurjchem-289	197	10	2.63	2.63	NUM
eurjchem-289	197	11	(	(	PUNCT
eurjchem-289	197	12	s	s	PROPN
eurjchem-289	197	13	,	,	PUNCT
eurjchem-289	197	14	3h	3h	NUM
eurjchem-289	197	15	,	,	PUNCT
eurjchem-289	197	16	ch3	ch3	PROPN
eurjchem-289	197	17	)	)	PUNCT
eurjchem-289	197	18	,	,	PUNCT
eurjchem-289	197	19	7.02‐7.78	7.02‐7.78	NUM
eurjchem-289	197	20	(	(	PUNCT
eurjchem-289	197	21	m	m	PROPN
eurjchem-289	197	22	,	,	PUNCT
eurjchem-289	197	23	9h	9h	NOUN
eurjchem-289	197	24	,	,	PUNCT
eurjchem-289	197	25	aromatic	aromatic	ADJ
eurjchem-289	197	26	protons	proton	NOUN
eurjchem-289	197	27	)	)	PUNCT
eurjchem-289	197	28	,	,	PUNCT
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eurjchem-289	197	30	,	,	PUNCT
eurjchem-289	197	31	13.38	13.38	NUM
eurjchem-289	197	32	(	(	PUNCT
eurjchem-289	197	33	2s	2s	NUM
eurjchem-289	197	34	,	,	PUNCT
eurjchem-289	197	35	2h	2h	NUM
eurjchem-289	197	36	,	,	PUNCT
eurjchem-289	197	37	2nh	2nh	NOUN
eurjchem-289	197	38	exchanged	exchange	VERB
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eurjchem-289	197	40	d2o	d2o	NOUN
eurjchem-289	197	41	)	)	PUNCT
eurjchem-289	197	42	.	.	PUNCT
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eurjchem-289	198	2	(	(	PUNCT
eurjchem-289	198	3	m	m	PROPN
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eurjchem-289	198	5	z	z	NOUN
eurjchem-289	198	6	(	(	PUNCT
eurjchem-289	198	7	%	%	NOUN
eurjchem-289	198	8	)	)	PUNCT
eurjchem-289	198	9	):	):	PUNCT
eurjchem-289	198	10	77	77	NUM
eurjchem-289	198	11	(	(	PUNCT
eurjchem-289	198	12	100	100	NUM
eurjchem-289	198	13	%	%	NOUN
eurjchem-289	198	14	)	)	PUNCT
eurjchem-289	198	15	,	,	PUNCT
eurjchem-289	198	16	306	306	NUM
eurjchem-289	198	17	(	(	PUNCT
eurjchem-289	198	18	m+	m+	NUM
eurjchem-289	198	19	.	.	PROPN
eurjchem-289	198	20	,	,	PUNCT
eurjchem-289	198	21	41.77	41.77	NUM
eurjchem-289	198	22	%	%	NOUN
eurjchem-289	198	23	)	)	PUNCT
eurjchem-289	198	24	,	,	PUNCT
eurjchem-289	198	25	307	307	NUM
eurjchem-289	198	26	(	(	PUNCT
eurjchem-289	198	27	m+1	m+1	X
eurjchem-289	198	28	┐	┐	NUM
eurjchem-289	198	29	+	+	NOUN
eurjchem-289	198	30	.	.	PROPN
eurjchem-289	198	31	,	,	PUNCT
eurjchem-289	198	32	9.06	9.06	NUM
eurjchem-289	198	33	%	%	NOUN
eurjchem-289	198	34	)	)	PUNCT
eurjchem-289	198	35	.	.	PUNCT
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eurjchem-289	199	4	.	.	PUNCT
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eurjchem-289	200	3	(	(	PUNCT
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eurjchem-289	200	5	):	):	PUNCT
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eurjchem-289	200	7	,	,	PUNCT
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eurjchem-289	200	9	;	;	PUNCT
eurjchem-289	200	10	h	h	NOUN
eurjchem-289	200	11	,	,	PUNCT
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eurjchem-289	200	13	;	;	PUNCT
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eurjchem-289	200	15	,	,	PUNCT
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eurjchem-289	200	19	:	:	PUNCT
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eurjchem-289	201	2	,	,	PUNCT
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eurjchem-289	202	1	3‐[1‐(2‐(4‐chlorophenyl)hydrazinylidene)‐2‐oxopropyl	3‐[1‐(2‐(4‐chlorophenyl)hydrazinylidene)‐2‐oxopropyl	NUM
eurjchem-289	202	2	]	]	PUNCT
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eurjchem-289	202	4	(	(	PUNCT
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eurjchem-289	202	6	):	):	PUNCT
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eurjchem-289	202	8	:	:	PUNCT
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eurjchem-289	202	10	%	%	NOUN
eurjchem-289	202	11	.	.	PUNCT
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eurjchem-289	203	3	:	:	PUNCT
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eurjchem-289	204	7	,	,	PUNCT
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eurjchem-289	204	9	):	):	PUNCT
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eurjchem-289	204	11	(	(	PUNCT
eurjchem-289	204	12	nh	nh	NOUN
eurjchem-289	204	13	)	)	PUNCT
eurjchem-289	204	14	,	,	PUNCT
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eurjchem-289	204	16	,	,	PUNCT
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eurjchem-289	204	20	=	=	NOUN
eurjchem-289	204	21	o	o	NOUN
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eurjchem-289	204	23	,	,	PUNCT
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eurjchem-289	204	25	(	(	PUNCT
eurjchem-289	204	26	ch3	ch3	PROPN
eurjchem-289	204	27	bending	bending	NOUN
eurjchem-289	204	28	)	)	PUNCT
eurjchem-289	204	29	.	.	PUNCT
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eurjchem-289	205	7	,	,	PUNCT
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eurjchem-289	205	9	5:1	5:1	NUM
eurjchem-289	205	10	)	)	PUNCT
eurjchem-289	205	11	,	,	PUNCT
eurjchem-289	205	12	δ	δ	PROPN
eurjchem-289	205	13	,	,	PUNCT
eurjchem-289	205	14	ppm	ppm	NOUN
eurjchem-289	205	15	):	):	PUNCT
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eurjchem-289	205	17	(	(	PUNCT
eurjchem-289	205	18	s	s	PROPN
eurjchem-289	205	19	,	,	PUNCT
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eurjchem-289	205	21	,	,	PUNCT
eurjchem-289	205	22	ch3	ch3	PROPN
eurjchem-289	205	23	)	)	PUNCT
eurjchem-289	205	24	,	,	PUNCT
eurjchem-289	205	25	7.55‐7.95	7.55‐7.95	NUM
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eurjchem-289	205	28	,	,	PUNCT
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eurjchem-289	206	6	(	(	PUNCT
eurjchem-289	206	7	%	%	NOUN
eurjchem-289	206	8	)	)	PUNCT
eurjchem-289	206	9	):	):	PUNCT
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eurjchem-289	206	17	)	)	PUNCT
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eurjchem-289	206	34	,	,	PUNCT
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eurjchem-289	206	36	%	%	NOUN
eurjchem-289	206	37	)	)	PUNCT
eurjchem-289	206	38	.	.	PUNCT
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eurjchem-289	207	4	.	.	PUNCT
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eurjchem-289	208	15	,	,	PUNCT
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eurjchem-289	208	19	:	:	PUNCT
eurjchem-289	209	1	c	c	X
eurjchem-289	209	2	,	,	PUNCT
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eurjchem-289	209	4	;	;	PUNCT
eurjchem-289	210	1	h	h	NOUN
eurjchem-289	210	2	,	,	PUNCT
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eurjchem-289	210	4	;	;	PUNCT
eurjchem-289	210	5	n	n	CCONJ
eurjchem-289	210	6	,	,	PUNCT
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eurjchem-289	210	8	%	%	NOUN
eurjchem-289	210	9	.	.	PUNCT
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eurjchem-289	211	2	.	.	PUNCT
eurjchem-289	212	1	3‐(4‐hydroxy‐1‐phenyl‐1h‐pyrazol‐3‐yl)quinoxalin‐	3‐(4‐hydroxy‐1‐phenyl‐1h‐pyrazol‐3‐yl)quinoxalin‐	NUM
eurjchem-289	212	2	2(1h)‐one	2(1h)‐one	NUM
eurjchem-289	212	3	(	(	PUNCT
eurjchem-289	212	4	12	12	NUM
eurjchem-289	212	5	)	)	PUNCT
eurjchem-289	212	6	to	to	ADP
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eurjchem-289	212	8	stirred	stir	VERB
eurjchem-289	212	9	solution	solution	NOUN
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eurjchem-289	212	11	11a	11a	NOUN
eurjchem-289	212	12	(	(	PUNCT
eurjchem-289	212	13	1.53	1.53	NUM
eurjchem-289	212	14	g	g	NOUN
eurjchem-289	212	15	,	,	PUNCT
eurjchem-289	212	16	0.005	0.005	NUM
eurjchem-289	212	17	mol	mol	NOUN
eurjchem-289	212	18	)	)	PUNCT
eurjchem-289	212	19	and	and	CCONJ
eurjchem-289	212	20	sodium	sodium	NOUN
eurjchem-289	212	21	acetate	acetate	NOUN
eurjchem-289	212	22	(	(	PUNCT
eurjchem-289	212	23	0.82	0.82	NUM
eurjchem-289	212	24	g	g	NOUN
eurjchem-289	212	25	,	,	PUNCT
eurjchem-289	212	26	0.01	0.01	NUM
eurjchem-289	212	27	mol	mol	NOUN
eurjchem-289	212	28	)	)	PUNCT
eurjchem-289	212	29	in	in	ADP
eurjchem-289	212	30	acetic	acetic	ADJ
eurjchem-289	212	31	acid	acid	NOUN
eurjchem-289	212	32	(	(	PUNCT
eurjchem-289	212	33	10	10	NUM
eurjchem-289	212	34	ml	ml	NOUN
eurjchem-289	212	35	)	)	PUNCT
eurjchem-289	212	36	,	,	PUNCT
eurjchem-289	212	37	bromine	bromine	NOUN
eurjchem-289	212	38	(	(	PUNCT
eurjchem-289	212	39	0.8	0.8	NUM
eurjchem-289	212	40	g	g	NOUN
eurjchem-289	212	41	,	,	PUNCT
eurjchem-289	212	42	0.005	0.005	NUM
eurjchem-289	212	43	mol	mol	NOUN
eurjchem-289	212	44	)	)	PUNCT
eurjchem-289	212	45	in	in	ADP
eurjchem-289	212	46	acetic	acetic	ADJ
eurjchem-289	212	47	acid	acid	NOUN
eurjchem-289	212	48	(	(	PUNCT
eurjchem-289	212	49	2.3	2.3	NUM
eurjchem-289	212	50	ml	ml	NOUN
eurjchem-289	212	51	)	)	PUNCT
eurjchem-289	212	52	was	be	AUX
eurjchem-289	212	53	added	add	VERB
eurjchem-289	212	54	dropwise	dropwise	NOUN
eurjchem-289	212	55	.	.	PUNCT
eurjchem-289	213	1	the	the	DET
eurjchem-289	213	2	reaction	reaction	NOUN
eurjchem-289	213	3	mixture	mixture	NOUN
eurjchem-289	213	4	was	be	AUX
eurjchem-289	213	5	stirred	stir	VERB
eurjchem-289	213	6	overnight	overnight	ADV
eurjchem-289	213	7	.	.	PUNCT
eurjchem-289	214	1	water	water	NOUN
eurjchem-289	214	2	(	(	PUNCT
eurjchem-289	214	3	20	20	NUM
eurjchem-289	214	4	ml	ml	NOUN
eurjchem-289	214	5	)	)	PUNCT
eurjchem-289	214	6	was	be	AUX
eurjchem-289	214	7	then	then	ADV
eurjchem-289	214	8	added	add	VERB
eurjchem-289	214	9	and	and	CCONJ
eurjchem-289	214	10	the	the	DET
eurjchem-289	214	11	solid	solid	ADJ
eurjchem-289	214	12	product	product	NOUN
eurjchem-289	214	13	was	be	AUX
eurjchem-289	214	14	filtered	filter	VERB
eurjchem-289	214	15	and	and	CCONJ
eurjchem-289	214	16	crystallized	crystallize	VERB
eurjchem-289	214	17	from	from	ADP
eurjchem-289	214	18	methanol	methanol	NOUN
eurjchem-289	214	19	(	(	PUNCT
eurjchem-289	214	20	scheme	scheme	NOUN
eurjchem-289	214	21	2	2	NUM
eurjchem-289	214	22	)	)	PUNCT
eurjchem-289	214	23	.	.	PUNCT
eurjchem-289	215	1	yield	yield	NOUN
eurjchem-289	215	2	:	:	PUNCT
eurjchem-289	215	3	55	55	NUM
eurjchem-289	215	4	%	%	NOUN
eurjchem-289	215	5	.	.	PUNCT
eurjchem-289	216	1	m.p	m.p	PROPN
eurjchem-289	216	2	.	.	PROPN
eurjchem-289	216	3	:	:	PUNCT
eurjchem-289	217	1	244‐246	244‐246	NUM
eurjchem-289	217	2	°	°	SYM
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eurjchem-289	217	4	.	.	PUNCT
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eurjchem-289	218	2	(	(	PUNCT
eurjchem-289	218	3	kbr	kbr	PROPN
eurjchem-289	218	4	,	,	PUNCT
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eurjchem-289	218	6	):	):	PUNCT
eurjchem-289	218	7	3500‐3350	3500‐3350	PROPN
eurjchem-289	218	8	(	(	PUNCT
eurjchem-289	218	9	nh	nh	PROPN
eurjchem-289	218	10	,	,	PUNCT
eurjchem-289	218	11	oh	oh	INTJ
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eurjchem-289	218	13	)	)	PUNCT
eurjchem-289	218	14	,	,	PUNCT
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eurjchem-289	218	16	(	(	PUNCT
eurjchem-289	218	17	c	c	NOUN
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eurjchem-289	218	21	)	)	PUNCT
eurjchem-289	218	22	.	.	PUNCT
eurjchem-289	219	1	1h	1h	NUM
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eurjchem-289	219	3	(	(	PUNCT
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eurjchem-289	219	5	,	,	PUNCT
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eurjchem-289	219	9	):	):	PUNCT
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eurjchem-289	219	11	(	(	PUNCT
eurjchem-289	219	12	m	m	PROPN
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eurjchem-289	219	18	)	)	PUNCT
eurjchem-289	219	19	,	,	PUNCT
eurjchem-289	219	20	11.04	11.04	NUM
eurjchem-289	219	21	,	,	PUNCT
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eurjchem-289	219	23	(	(	PUNCT
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eurjchem-289	219	25	,	,	PUNCT
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eurjchem-289	219	27	,	,	PUNCT
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eurjchem-289	219	34	d2o	d2o	NOUN
eurjchem-289	219	35	)	)	PUNCT
eurjchem-289	219	36	.	.	PUNCT
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eurjchem-289	220	6	(	(	PUNCT
eurjchem-289	220	7	%	%	NOUN
eurjchem-289	220	8	)	)	PUNCT
eurjchem-289	220	9	):	):	PUNCT
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eurjchem-289	220	11	(	(	PUNCT
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eurjchem-289	220	14	)	)	PUNCT
eurjchem-289	220	15	,	,	PUNCT
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eurjchem-289	220	17	(	(	PUNCT
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eurjchem-289	220	20	,	,	PUNCT
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eurjchem-289	220	22	%	%	NOUN
eurjchem-289	220	23	)	)	PUNCT
eurjchem-289	220	24	,	,	PUNCT
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eurjchem-289	220	35	.	.	PUNCT
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eurjchem-289	221	4	.	.	PUNCT
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eurjchem-289	222	7	,	,	PUNCT
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eurjchem-289	224	2	,	,	PUNCT
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eurjchem-289	224	10	,	,	PUNCT
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eurjchem-289	224	13	.	.	PUNCT
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eurjchem-289	225	2	.	.	X
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eurjchem-289	225	4	(	(	PUNCT
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eurjchem-289	225	11	(	(	PUNCT
eurjchem-289	225	12	1.01	1.01	NUM
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eurjchem-289	225	14	,	,	PUNCT
eurjchem-289	225	15	0.005	0.005	NUM
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eurjchem-289	225	22	(	(	PUNCT
eurjchem-289	225	23	25	25	NUM
eurjchem-289	225	24	ml	ml	NOUN
eurjchem-289	225	25	)	)	PUNCT
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eurjchem-289	225	28	at	at	ADP
eurjchem-289	225	29	room	room	NOUN
eurjchem-289	225	30	temperature	temperature	NOUN
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eurjchem-289	225	32	5	5	NUM
eurjchem-289	225	33	min	min	NOUN
eurjchem-289	225	34	;	;	PUNCT
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eurjchem-289	225	39	°	°	PROPN
eurjchem-289	225	40	c	c	NOUN
eurjchem-289	225	41	.	.	PUNCT
eurjchem-289	226	1	to	to	ADP
eurjchem-289	226	2	this	this	DET
eurjchem-289	226	3	solution	solution	NOUN
eurjchem-289	226	4	solid	solid	ADJ
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eurjchem-289	226	6	nitrite	nitrite	NOUN
eurjchem-289	226	7	(	(	PUNCT
eurjchem-289	226	8	0.48	0.48	NUM
eurjchem-289	226	9	g	g	NOUN
eurjchem-289	226	10	,	,	PUNCT
eurjchem-289	226	11	0.007	0.007	NUM
eurjchem-289	226	12	mol	mol	NOUN
eurjchem-289	226	13	)	)	PUNCT
eurjchem-289	226	14	was	be	AUX
eurjchem-289	226	15	added	add	VERB
eurjchem-289	226	16	portionwise	portionwise	ADV
eurjchem-289	226	17	over	over	ADP
eurjchem-289	226	18	a	a	DET
eurjchem-289	226	19	period	period	NOUN
eurjchem-289	226	20	of	of	ADP
eurjchem-289	226	21	30	30	NUM
eurjchem-289	226	22	min	min	NOUN
eurjchem-289	226	23	.	.	NOUN
eurjchem-289	226	24	after	after	ADP
eurjchem-289	226	25	stirring	stir	VERB
eurjchem-289	226	26	for	for	ADP
eurjchem-289	226	27	an	an	DET
eurjchem-289	226	28	additional	additional	ADJ
eurjchem-289	226	29	30	30	NUM
eurjchem-289	226	30	min	min	NOUN
eurjchem-289	226	31	at	at	ADP
eurjchem-289	226	32	room	room	NOUN
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eurjchem-289	226	36	reaction	reaction	NOUN
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eurjchem-289	226	38	was	be	AUX
eurjchem-289	226	39	diluted	dilute	VERB
eurjchem-289	226	40	with	with	ADP
eurjchem-289	226	41	water	water	NOUN
eurjchem-289	226	42	,	,	PUNCT
eurjchem-289	226	43	and	and	CCONJ
eurjchem-289	226	44	then	then	ADV
eurjchem-289	226	45	filtered	filter	VERB
eurjchem-289	226	46	.	.	PUNCT
eurjchem-289	227	1	the	the	DET
eurjchem-289	227	2	obtained	obtain	VERB
eurjchem-289	227	3	solid	solid	NOUN
eurjchem-289	227	4	was	be	AUX
eurjchem-289	227	5	washed	wash	VERB
eurjchem-289	227	6	with	with	ADP
eurjchem-289	227	7	water	water	NOUN
eurjchem-289	227	8	and	and	CCONJ
eurjchem-289	227	9	crystallized	crystallize	VERB
eurjchem-289	227	10	from	from	ADP
eurjchem-289	227	11	ethanol	ethanol	NOUN
eurjchem-289	227	12	(	(	PUNCT
eurjchem-289	227	13	scheme	scheme	NOUN
eurjchem-289	227	14	3	3	NUM
eurjchem-289	227	15	)	)	PUNCT
eurjchem-289	227	16	.	.	PUNCT
eurjchem-289	228	1	yield	yield	NOUN
eurjchem-289	228	2	:	:	PUNCT
eurjchem-289	228	3	90	90	NUM
eurjchem-289	228	4	%	%	NOUN
eurjchem-289	228	5	.	.	PUNCT
eurjchem-289	229	1	m.p	m.p	PROPN
eurjchem-289	229	2	.	.	PROPN
eurjchem-289	229	3	:	:	PUNCT
eurjchem-289	230	1	236‐238	236‐238	NUM
eurjchem-289	230	2	°	°	PROPN
eurjchem-289	230	3	c	c	NOUN
eurjchem-289	230	4	.	.	PUNCT
eurjchem-289	231	1	ir	ir	PROPN
eurjchem-289	231	2	(	(	PUNCT
eurjchem-289	231	3	kbr	kbr	PROPN
eurjchem-289	231	4	,	,	PUNCT
eurjchem-289	231	5	cm‐1	cm‐1	PROPN
eurjchem-289	231	6	):	):	PUNCT
eurjchem-289	231	7	3200‐	3200‐	NUM
eurjchem-289	231	8	3150	3150	NUM
eurjchem-289	231	9	(	(	PUNCT
eurjchem-289	231	10	nh	nh	PROPN
eurjchem-289	231	11	,	,	PUNCT
eurjchem-289	231	12	oh	oh	INTJ
eurjchem-289	231	13	stretching	stretching	NOUN
eurjchem-289	231	14	)	)	PUNCT
eurjchem-289	231	15	,	,	PUNCT
eurjchem-289	231	16	1690	1690	NUM
eurjchem-289	231	17	,	,	PUNCT
eurjchem-289	231	18	1660	1660	NUM
eurjchem-289	231	19	(	(	PUNCT
eurjchem-289	231	20	c	c	NOUN
eurjchem-289	231	21	=	=	NOUN
eurjchem-289	231	22	o	o	NOUN
eurjchem-289	231	23	stretching	stretching	NOUN
eurjchem-289	231	24	)	)	PUNCT
eurjchem-289	231	25	,	,	PUNCT
eurjchem-289	231	26	1370	1370	NUM
eurjchem-289	231	27	(	(	PUNCT
eurjchem-289	231	28	ch3	ch3	PROPN
eurjchem-289	231	29	bending	bending	NOUN
eurjchem-289	231	30	)	)	PUNCT
eurjchem-289	231	31	.	.	PUNCT
eurjchem-289	232	1	1h	1h	NUM
eurjchem-289	232	2	nmr	nmr	NOUN
eurjchem-289	232	3	(	(	PUNCT
eurjchem-289	232	4	dmso‐d6	dmso‐d6	PROPN
eurjchem-289	232	5	,	,	PUNCT
eurjchem-289	232	6	δ	δ	PROPN
eurjchem-289	232	7	,	,	PUNCT
eurjchem-289	232	8	ppm	ppm	NUM
eurjchem-289	232	9	):	):	PUNCT
eurjchem-289	232	10	2.49	2.49	NUM
eurjchem-289	232	11	(	(	PUNCT
eurjchem-289	232	12	s	s	PROPN
eurjchem-289	232	13	,	,	PUNCT
eurjchem-289	232	14	ch3	ch3	PROPN
eurjchem-289	232	15	,	,	PUNCT
eurjchem-289	232	16	3h	3h	NUM
eurjchem-289	232	17	)	)	PUNCT
eurjchem-289	232	18	,	,	PUNCT
eurjchem-289	232	19	7.31‐7.80	7.31‐7.80	NUM
eurjchem-289	232	20	(	(	PUNCT
eurjchem-289	232	21	m	m	PROPN
eurjchem-289	232	22	,	,	PUNCT
eurjchem-289	232	23	4h	4h	NUM
eurjchem-289	232	24	,	,	PUNCT
eurjchem-289	232	25	aromatic	aromatic	ADJ
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eurjchem-289	232	27	)	)	PUNCT
eurjchem-289	232	28	,	,	PUNCT
eurjchem-289	232	29	12.61	12.61	NUM
eurjchem-289	232	30	,	,	PUNCT
eurjchem-289	232	31	12.87	12.87	NUM
eurjchem-289	232	32	(	(	PUNCT
eurjchem-289	232	33	2s	2s	NUM
eurjchem-289	232	34	,	,	PUNCT
eurjchem-289	232	35	2h	2h	NUM
eurjchem-289	232	36	,	,	PUNCT
eurjchem-289	232	37	nh	nh	PROPN
eurjchem-289	232	38	,	,	PUNCT
eurjchem-289	232	39	oh	oh	INTJ
eurjchem-289	232	40	exchanged	exchange	VERB
eurjchem-289	232	41	with	with	ADP
eurjchem-289	232	42	d2o	d2o	NOUN
eurjchem-289	232	43	)	)	PUNCT
eurjchem-289	232	44	.	.	PUNCT
eurjchem-289	233	1	ms	ms	NOUN
eurjchem-289	233	2	(	(	PUNCT
eurjchem-289	233	3	m	m	PROPN
eurjchem-289	233	4	/	/	SYM
eurjchem-289	233	5	z	z	NOUN
eurjchem-289	233	6	(	(	PUNCT
eurjchem-289	233	7	%	%	NOUN
eurjchem-289	233	8	)	)	PUNCT
eurjchem-289	233	9	):	):	PUNCT
eurjchem-289	233	10	172	172	NUM
eurjchem-289	233	11	(	(	PUNCT
eurjchem-289	233	12	100	100	NUM
eurjchem-289	233	13	%	%	NOUN
eurjchem-289	233	14	)	)	PUNCT
eurjchem-289	233	15	,	,	PUNCT
eurjchem-289	233	16	231	231	NUM
eurjchem-289	233	17	(	(	PUNCT
eurjchem-289	233	18	m+	m+	NUM
eurjchem-289	233	19	.	.	PROPN
eurjchem-289	233	20	,	,	PUNCT
eurjchem-289	233	21	29.28	29.28	NUM
eurjchem-289	233	22	%	%	NOUN
eurjchem-289	233	23	)	)	PUNCT
eurjchem-289	233	24	,	,	PUNCT
eurjchem-289	233	25	232(m+1	232(m+1	PROPN
eurjchem-289	233	26	┐	┐	PROPN
eurjchem-289	233	27	+	+	PROPN
eurjchem-289	233	28	.	.	PROPN
eurjchem-289	233	29	,	,	PUNCT
eurjchem-289	233	30	4.22	4.22	NUM
eurjchem-289	233	31	%	%	NOUN
eurjchem-289	233	32	)	)	PUNCT
eurjchem-289	233	33	.	.	PUNCT
eurjchem-289	234	1	anal	anal	PROPN
eurjchem-289	234	2	.	.	PUNCT
eurjchem-289	235	1	cald	cald	PROPN
eurjchem-289	235	2	.	.	PUNCT
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eurjchem-289	236	2	c11h9n3o3	c11h9n3o3	NOUN
eurjchem-289	236	3	(	(	PUNCT
eurjchem-289	236	4	231	231	NUM
eurjchem-289	236	5	):	):	PUNCT
eurjchem-289	236	6	c	c	NOUN
eurjchem-289	236	7	,	,	PUNCT
eurjchem-289	236	8	57.14	57.14	NUM
eurjchem-289	236	9	;	;	PUNCT
eurjchem-289	236	10	h	h	NOUN
eurjchem-289	236	11	,	,	PUNCT
eurjchem-289	236	12	3.89	3.89	NUM
eurjchem-289	236	13	;	;	PUNCT
eurjchem-289	236	14	n	n	PRON
eurjchem-289	236	15	18.18	18.18	NUM
eurjchem-289	236	16	.	.	PUNCT
eurjchem-289	236	17	found	find	VERB
eurjchem-289	236	18	:	:	PUNCT
eurjchem-289	237	1	c	c	X
eurjchem-289	237	2	,	,	PUNCT
eurjchem-289	237	3	57.40	57.40	NUM
eurjchem-289	237	4	;	;	PUNCT
eurjchem-289	237	5	h	h	NOUN
eurjchem-289	237	6	,	,	PUNCT
eurjchem-289	237	7	3.90	3.90	NUM
eurjchem-289	237	8	;	;	PUNCT
eurjchem-289	237	9	n	n	CCONJ
eurjchem-289	237	10	,	,	PUNCT
eurjchem-289	237	11	18.06	18.06	NUM
eurjchem-289	237	12	%	%	NOUN
eurjchem-289	237	13	.	.	PUNCT
eurjchem-289	238	1	shabaan	shabaan	X
eurjchem-289	238	2	et	et	PROPN
eurjchem-289	238	3	al	al	PROPN
eurjchem-289	238	4	.	.	PUNCT
eurjchem-289	238	5	/	/	SYM
eurjchem-289	238	6	european	european	PROPN
eurjchem-289	238	7	journal	journal	PROPN
eurjchem-289	238	8	of	of	ADP
eurjchem-289	238	9	chemistry	chemistry	NOUN
eurjchem-289	238	10	2	2	NUM
eurjchem-289	238	11	(	(	PUNCT
eurjchem-289	238	12	3	3	NUM
eurjchem-289	238	13	)	)	PUNCT
eurjchem-289	238	14	(	(	PUNCT
eurjchem-289	238	15	2011	2011	NUM
eurjchem-289	238	16	)	)	PUNCT
eurjchem-289	239	1	365‐371	365‐371	NUM
eurjchem-289	239	2	369	369	NUM
eurjchem-289	239	3	n	n	PRON
eurjchem-289	239	4	h	h	NOUN
eurjchem-289	239	5	n	n	ADV
eurjchem-289	239	6	o	o	NOUN
eurjchem-289	239	7	o	o	NOUN
eurjchem-289	239	8	n	n	CCONJ
eurjchem-289	239	9	h	h	NOUN
eurjchem-289	239	10	n	n	ADV
eurjchem-289	239	11	o	o	NOUN
eurjchem-289	239	12	o	o	NOUN
eurjchem-289	239	13	n	n	INTJ
eurjchem-289	240	1	oh	oh	INTJ
eurjchem-289	240	2	n	n	ADV
eurjchem-289	240	3	h	h	NOUN
eurjchem-289	240	4	n	n	ADV
eurjchem-289	241	1	oh	oh	INTJ
eurjchem-289	241	2	o	o	INTJ
eurjchem-289	241	3	hn	hn	PRON
eurjchem-289	241	4	o	o	PROPN
eurjchem-289	241	5	ar	ar	PROPN
eurjchem-289	241	6	sodium	sodium	NOUN
eurjchem-289	241	7	nitrite	nitrite	NOUN
eurjchem-289	241	8	acetic	acetic	ADJ
eurjchem-289	241	9	acid	acid	PROPN
eurjchem-289	241	10	archo	archo	PROPN
eurjchem-289	241	11	naoh	naoh	PROPN
eurjchem-289	241	12	14a	14a	PROPN
eurjchem-289	241	13	,	,	PUNCT
eurjchem-289	241	14	b	b	PROPN
eurjchem-289	241	15	2	2	NUM
eurjchem-289	241	16	13	13	NUM
eurjchem-289	241	17	ar	ar	NOUN
eurjchem-289	241	18	=	=	PROPN
eurjchem-289	241	19	c6h5	c6h5	PROPN
eurjchem-289	241	20	,	,	PUNCT
eurjchem-289	241	21	p	p	ADJ
eurjchem-289	241	22	-	-	PUNCT
eurjchem-289	241	23	brc6h4	brc6h4	NOUN
eurjchem-289	241	24	scheme	scheme	NOUN
eurjchem-289	241	25	3	3	NUM
eurjchem-289	241	26	2.2.13	2.2.13	NUM
eurjchem-289	241	27	.	.	PUNCT
eurjchem-289	242	1	3‐(6‐aryl‐4‐hydroxy‐2h‐1,2‐oxazin‐3‐yl)quinoxalin‐	3‐(6‐aryl‐4‐hydroxy‐2h‐1,2‐oxazin‐3‐yl)quinoxalin‐	NUM
eurjchem-289	242	2	2(1h)‐ones	2(1h)‐ones	NUM
eurjchem-289	242	3	(	(	PUNCT
eurjchem-289	242	4	14a	14a	NOUN
eurjchem-289	242	5	,	,	PUNCT
eurjchem-289	242	6	b	b	NOUN
eurjchem-289	242	7	)	)	PUNCT
eurjchem-289	242	8	to	to	ADP
eurjchem-289	242	9	a	a	DET
eurjchem-289	242	10	suspension	suspension	NOUN
eurjchem-289	242	11	of	of	ADP
eurjchem-289	242	12	13	13	NUM
eurjchem-289	242	13	(	(	PUNCT
eurjchem-289	242	14	0.46	0.46	NUM
eurjchem-289	242	15	g	g	NOUN
eurjchem-289	242	16	,	,	PUNCT
eurjchem-289	242	17	0.002	0.002	NUM
eurjchem-289	242	18	mol	mol	NOUN
eurjchem-289	242	19	)	)	PUNCT
eurjchem-289	242	20	in	in	ADP
eurjchem-289	242	21	water	water	NOUN
eurjchem-289	242	22	(	(	PUNCT
eurjchem-289	242	23	10	10	NUM
eurjchem-289	242	24	ml	ml	NOUN
eurjchem-289	242	25	)	)	PUNCT
eurjchem-289	242	26	,	,	PUNCT
eurjchem-289	242	27	10	10	NUM
eurjchem-289	242	28	%	%	NOUN
eurjchem-289	242	29	aqueous	aqueous	ADJ
eurjchem-289	242	30	sodium	sodium	NOUN
eurjchem-289	242	31	hydroxide	hydroxide	NOUN
eurjchem-289	242	32	(	(	PUNCT
eurjchem-289	242	33	2	2	NUM
eurjchem-289	242	34	ml	ml	NOUN
eurjchem-289	242	35	)	)	PUNCT
eurjchem-289	242	36	solution	solution	NOUN
eurjchem-289	242	37	and	and	CCONJ
eurjchem-289	242	38	the	the	DET
eurjchem-289	242	39	appropriate	appropriate	ADJ
eurjchem-289	242	40	aldehyde	aldehyde	NOUN
eurjchem-289	242	41	(	(	PUNCT
eurjchem-289	242	42	0.002	0.002	NUM
eurjchem-289	242	43	mol	mol	NOUN
eurjchem-289	242	44	)	)	PUNCT
eurjchem-289	242	45	were	be	AUX
eurjchem-289	242	46	sequentially	sequentially	ADV
eurjchem-289	242	47	added	add	VERB
eurjchem-289	242	48	.	.	PUNCT
eurjchem-289	243	1	the	the	DET
eurjchem-289	243	2	reaction	reaction	NOUN
eurjchem-289	243	3	mixture	mixture	NOUN
eurjchem-289	243	4	was	be	AUX
eurjchem-289	243	5	heated	heat	VERB
eurjchem-289	243	6	under	under	ADP
eurjchem-289	243	7	reflux	reflux	NOUN
eurjchem-289	243	8	for	for	ADP
eurjchem-289	243	9	5	5	NUM
eurjchem-289	243	10	h.	h.	NOUN
eurjchem-289	243	11	the	the	DET
eurjchem-289	243	12	formed	form	VERB
eurjchem-289	243	13	solid	solid	ADJ
eurjchem-289	243	14	was	be	AUX
eurjchem-289	243	15	filtered	filter	VERB
eurjchem-289	243	16	,	,	PUNCT
eurjchem-289	243	17	washed	wash	VERB
eurjchem-289	243	18	with	with	ADP
eurjchem-289	243	19	ethanol	ethanol	NOUN
eurjchem-289	243	20	and	and	CCONJ
eurjchem-289	243	21	crystallized	crystallize	VERB
eurjchem-289	243	22	from	from	ADP
eurjchem-289	243	23	methanol	methanol	NOUN
eurjchem-289	243	24	(	(	PUNCT
eurjchem-289	243	25	scheme	scheme	NOUN
eurjchem-289	243	26	3	3	NUM
eurjchem-289	243	27	)	)	PUNCT
eurjchem-289	243	28	.	.	PUNCT
eurjchem-289	244	1	3‐(6‐phenyl‐4‐hydroxy‐2h‐1,2‐oxazin‐3‐yl)quinoxalin‐2(1h)‐	3‐(6‐phenyl‐4‐hydroxy‐2h‐1,2‐oxazin‐3‐yl)quinoxalin‐2(1h)‐	NUM
eurjchem-289	244	2	ones	one	NOUN
eurjchem-289	244	3	(	(	PUNCT
eurjchem-289	244	4	14a	14a	NOUN
eurjchem-289	244	5	):	):	PUNCT
eurjchem-289	244	6	yield	yield	NOUN
eurjchem-289	244	7	:	:	PUNCT
eurjchem-289	244	8	60	60	NUM
eurjchem-289	244	9	%	%	NOUN
eurjchem-289	244	10	.	.	PUNCT
eurjchem-289	245	1	m.p	m.p	PROPN
eurjchem-289	245	2	.	.	PROPN
eurjchem-289	245	3	:	:	PUNCT
eurjchem-289	246	1	285‐287	285‐287	NUM
eurjchem-289	246	2	°	°	SYM
eurjchem-289	246	3	c	c	X
eurjchem-289	246	4	.	.	PUNCT
eurjchem-289	247	1	ir	ir	PROPN
eurjchem-289	247	2	(	(	PUNCT
eurjchem-289	247	3	kbr	kbr	PROPN
eurjchem-289	247	4	,	,	PUNCT
eurjchem-289	247	5	cm‐1	cm‐1	PROPN
eurjchem-289	247	6	):	):	PUNCT
eurjchem-289	247	7	3600‐	3600‐	NUM
eurjchem-289	247	8	3400	3400	NUM
eurjchem-289	247	9	(	(	PUNCT
eurjchem-289	247	10	nh	nh	PROPN
eurjchem-289	247	11	,	,	PUNCT
eurjchem-289	247	12	oh	oh	INTJ
eurjchem-289	247	13	stretching	stretching	NOUN
eurjchem-289	247	14	)	)	PUNCT
eurjchem-289	247	15	,	,	PUNCT
eurjchem-289	247	16	1660	1660	NUM
eurjchem-289	247	17	(	(	PUNCT
eurjchem-289	247	18	c	c	NOUN
eurjchem-289	247	19	=	=	NOUN
eurjchem-289	247	20	o	o	NOUN
eurjchem-289	247	21	stretching	stretching	NOUN
eurjchem-289	247	22	)	)	PUNCT
eurjchem-289	247	23	.	.	PUNCT
eurjchem-289	248	1	1h	1h	NUM
eurjchem-289	248	2	nmr	nmr	NOUN
eurjchem-289	248	3	(	(	PUNCT
eurjchem-289	248	4	dmso‐d6	dmso‐d6	PROPN
eurjchem-289	248	5	,	,	PUNCT
eurjchem-289	248	6	δ	δ	PROPN
eurjchem-289	248	7	,	,	PUNCT
eurjchem-289	248	8	ppm	ppm	NUM
eurjchem-289	248	9	):	):	PUNCT
eurjchem-289	248	10	6.37	6.37	NUM
eurjchem-289	248	11	(	(	PUNCT
eurjchem-289	248	12	s	s	PROPN
eurjchem-289	248	13	,	,	PUNCT
eurjchem-289	248	14	1h	1h	NUM
eurjchem-289	248	15	,	,	PUNCT
eurjchem-289	248	16	ch	ch	NOUN
eurjchem-289	248	17	of	of	ADP
eurjchem-289	248	18	oxazine	oxazine	NOUN
eurjchem-289	248	19	)	)	PUNCT
eurjchem-289	248	20	,	,	PUNCT
eurjchem-289	248	21	7.35‐7.78	7.35‐7.78	PROPN
eurjchem-289	248	22	(	(	PUNCT
eurjchem-289	248	23	m	m	PROPN
eurjchem-289	248	24	,	,	PUNCT
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eurjchem-289	248	26	,	,	PUNCT
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eurjchem-289	248	28	protons	proton	NOUN
eurjchem-289	248	29	)	)	PUNCT
eurjchem-289	248	30	,	,	PUNCT
eurjchem-289	248	31	7.91	7.91	NUM
eurjchem-289	248	32	,	,	PUNCT
eurjchem-289	248	33	10.66	10.66	NUM
eurjchem-289	248	34	,	,	PUNCT
eurjchem-289	248	35	12.03	12.03	NUM
eurjchem-289	248	36	(	(	PUNCT
eurjchem-289	248	37	3s	3s	NOUN
eurjchem-289	248	38	,	,	PUNCT
eurjchem-289	248	39	3h	3h	NUM
eurjchem-289	248	40	,	,	PUNCT
eurjchem-289	248	41	nh	nh	PROPN
eurjchem-289	248	42	,	,	PUNCT
eurjchem-289	248	43	oh	oh	INTJ
eurjchem-289	248	44	,	,	PUNCT
eurjchem-289	248	45	exchanged	exchange	VERB
eurjchem-289	248	46	with	with	ADP
eurjchem-289	248	47	d2o	d2o	NOUN
eurjchem-289	248	48	)	)	PUNCT
eurjchem-289	248	49	.	.	PUNCT
eurjchem-289	249	1	ms	ms	NOUN
eurjchem-289	249	2	(	(	PUNCT
eurjchem-289	249	3	m	m	PROPN
eurjchem-289	249	4	/	/	SYM
eurjchem-289	249	5	z	z	NOUN
eurjchem-289	249	6	(	(	PUNCT
eurjchem-289	249	7	%	%	NOUN
eurjchem-289	249	8	)	)	PUNCT
eurjchem-289	249	9	):	):	PUNCT
eurjchem-289	249	10	303	303	NUM
eurjchem-289	249	11	(	(	PUNCT
eurjchem-289	249	12	100	100	NUM
eurjchem-289	249	13	%	%	NOUN
eurjchem-289	249	14	)	)	PUNCT
eurjchem-289	249	15	,	,	PUNCT
eurjchem-289	249	16	319	319	NUM
eurjchem-289	249	17	(	(	PUNCT
eurjchem-289	249	18	m+	m+	NUM
eurjchem-289	249	19	.	.	PROPN
eurjchem-289	249	20	,	,	PUNCT
eurjchem-289	249	21	0.4	0.4	NUM
eurjchem-289	249	22	%	%	NOUN
eurjchem-289	249	23	)	)	PUNCT
eurjchem-289	249	24	.	.	PUNCT
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eurjchem-289	250	2	.	.	PUNCT
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eurjchem-289	250	4	.	.	PUNCT
eurjchem-289	251	1	for	for	ADP
eurjchem-289	251	2	c18h13n3o3	c18h13n3o3	NUM
eurjchem-289	251	3	(	(	PUNCT
eurjchem-289	251	4	319	319	NUM
eurjchem-289	251	5	):	):	PUNCT
eurjchem-289	251	6	c	c	NOUN
eurjchem-289	251	7	,	,	PUNCT
eurjchem-289	251	8	67.71	67.71	NUM
eurjchem-289	251	9	;	;	PUNCT
eurjchem-289	251	10	h	h	X
eurjchem-289	251	11	,	,	PUNCT
eurjchem-289	251	12	4.07	4.07	NUM
eurjchem-289	251	13	;	;	PUNCT
eurjchem-289	251	14	n	n	CCONJ
eurjchem-289	251	15	,	,	PUNCT
eurjchem-289	251	16	13.16	13.16	NUM
eurjchem-289	251	17	.	.	PUNCT
eurjchem-289	252	1	found	find	VERB
eurjchem-289	252	2	:	:	PUNCT
eurjchem-289	253	1	c	c	X
eurjchem-289	253	2	,	,	PUNCT
eurjchem-289	253	3	67.58	67.58	NUM
eurjchem-289	253	4	;	;	PUNCT
eurjchem-289	253	5	h	h	NOUN
eurjchem-289	253	6	,	,	PUNCT
eurjchem-289	253	7	3.91	3.91	NUM
eurjchem-289	253	8	;	;	PUNCT
eurjchem-289	253	9	n	n	CCONJ
eurjchem-289	253	10	,	,	PUNCT
eurjchem-289	253	11	13.33	13.33	NUM
eurjchem-289	253	12	%	%	NOUN
eurjchem-289	253	13	.	.	PUNCT
eurjchem-289	254	1	3‐(6‐(4‐bromophenyl)‐4‐hydroxy‐2h‐1,2‐oxazin‐3‐yl	3‐(6‐(4‐bromophenyl)‐4‐hydroxy‐2h‐1,2‐oxazin‐3‐yl	NUM
eurjchem-289	254	2	)	)	PUNCT
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eurjchem-289	254	4	(	(	PUNCT
eurjchem-289	254	5	14b	14b	NUM
eurjchem-289	254	6	):	):	PUNCT
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eurjchem-289	254	8	:	:	PUNCT
eurjchem-289	254	9	43	43	NUM
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eurjchem-289	255	3	:	:	PUNCT
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eurjchem-289	256	2	°	°	PROPN
eurjchem-289	256	3	c	c	X
eurjchem-289	256	4	.	.	PUNCT
eurjchem-289	257	1	ir	ir	PROPN
eurjchem-289	257	2	(	(	PUNCT
eurjchem-289	257	3	kbr	kbr	PROPN
eurjchem-289	257	4	,	,	PUNCT
eurjchem-289	257	5	cm‐1	cm‐1	PROPN
eurjchem-289	257	6	):	):	PUNCT
eurjchem-289	257	7	3400‐3300	3400‐3300	NUM
eurjchem-289	257	8	(	(	PUNCT
eurjchem-289	257	9	nh	nh	PROPN
eurjchem-289	257	10	,	,	PUNCT
eurjchem-289	257	11	oh	oh	INTJ
eurjchem-289	257	12	stretching	stretching	NOUN
eurjchem-289	257	13	)	)	PUNCT
eurjchem-289	257	14	,	,	PUNCT
eurjchem-289	257	15	1670	1670	NUM
eurjchem-289	257	16	(	(	PUNCT
eurjchem-289	257	17	c	c	NOUN
eurjchem-289	257	18	=	=	NOUN
eurjchem-289	257	19	o	o	NOUN
eurjchem-289	257	20	stretching	stretching	NOUN
eurjchem-289	257	21	)	)	PUNCT
eurjchem-289	257	22	.	.	PUNCT
eurjchem-289	258	1	1h	1h	NUM
eurjchem-289	258	2	nmr	nmr	NOUN
eurjchem-289	258	3	(	(	PUNCT
eurjchem-289	258	4	dmso‐d6	dmso‐d6	PROPN
eurjchem-289	258	5	,	,	PUNCT
eurjchem-289	258	6	δ	δ	PROPN
eurjchem-289	258	7	,	,	PUNCT
eurjchem-289	258	8	ppm	ppm	NUM
eurjchem-289	258	9	):	):	PUNCT
eurjchem-289	258	10	6.00	6.00	NUM
eurjchem-289	258	11	(	(	PUNCT
eurjchem-289	258	12	s	s	PROPN
eurjchem-289	258	13	,	,	PUNCT
eurjchem-289	258	14	1h	1h	NUM
eurjchem-289	258	15	,	,	PUNCT
eurjchem-289	258	16	ch	ch	NOUN
eurjchem-289	258	17	of	of	ADP
eurjchem-289	258	18	oxazine	oxazine	NOUN
eurjchem-289	258	19	)	)	PUNCT
eurjchem-289	258	20	,	,	PUNCT
eurjchem-289	258	21	6.88‐7.69	6.88‐7.69	NUM
eurjchem-289	258	22	(	(	PUNCT
eurjchem-289	258	23	m	m	PROPN
eurjchem-289	258	24	,	,	PUNCT
eurjchem-289	258	25	8h	8h	NUM
eurjchem-289	258	26	,	,	PUNCT
eurjchem-289	258	27	aromatic	aromatic	ADJ
eurjchem-289	258	28	protons	proton	NOUN
eurjchem-289	258	29	)	)	PUNCT
eurjchem-289	258	30	.	.	PUNCT
eurjchem-289	259	1	anal	anal	PROPN
eurjchem-289	259	2	.	.	PUNCT
eurjchem-289	259	3	calcd	calcd	NOUN
eurjchem-289	259	4	.	.	PUNCT
eurjchem-289	260	1	for	for	SCONJ
eurjchem-289	260	2	c18h12brn3o3	c18h12brn3o3	NOUN
eurjchem-289	260	3	(	(	PUNCT
eurjchem-289	260	4	398	398	NUM
eurjchem-289	260	5	):	):	PUNCT
eurjchem-289	260	6	c	c	X
eurjchem-289	260	7	,	,	PUNCT
eurjchem-289	260	8	54.27	54.27	NUM
eurjchem-289	260	9	;	;	PUNCT
eurjchem-289	260	10	h	h	NOUN
eurjchem-289	260	11	,	,	PUNCT
eurjchem-289	260	12	3.01	3.01	NUM
eurjchem-289	260	13	;	;	PUNCT
eurjchem-289	260	14	n	n	CCONJ
eurjchem-289	260	15	,	,	PUNCT
eurjchem-289	260	16	10.55	10.55	NUM
eurjchem-289	260	17	.	.	PUNCT
eurjchem-289	260	18	found	find	VERB
eurjchem-289	260	19	:	:	PUNCT
eurjchem-289	261	1	c	c	X
eurjchem-289	261	2	,	,	PUNCT
eurjchem-289	261	3	54.29	54.29	NUM
eurjchem-289	261	4	;	;	PUNCT
eurjchem-289	261	5	h	h	NOUN
eurjchem-289	261	6	,	,	PUNCT
eurjchem-289	261	7	2.92	2.92	NUM
eurjchem-289	261	8	;	;	PUNCT
eurjchem-289	261	9	n	n	CCONJ
eurjchem-289	261	10	,	,	PUNCT
eurjchem-289	261	11	10.90	10.90	NUM
eurjchem-289	261	12	%	%	NOUN
eurjchem-289	261	13	.	.	PUNCT
eurjchem-289	262	1	2.3	2.3	NUM
eurjchem-289	262	2	.	.	PUNCT
eurjchem-289	263	1	microbiology	microbiology	NOUN
eurjchem-289	263	2	test	test	NOUN
eurjchem-289	263	3	2.3.1	2.3.1	NUM
eurjchem-289	263	4	.	.	PUNCT
eurjchem-289	263	5	test	test	NOUN
eurjchem-289	263	6	organisms	organism	NOUN
eurjchem-289	263	7	and	and	CCONJ
eurjchem-289	263	8	culture	culture	NOUN
eurjchem-289	263	9	media	medium	NOUN
eurjchem-289	263	10	twelve	twelve	NUM
eurjchem-289	263	11	compounds	compound	NOUN
eurjchem-289	263	12	were	be	AUX
eurjchem-289	263	13	tested	test	VERB
eurjchem-289	263	14	for	for	ADP
eurjchem-289	263	15	their	their	PRON
eurjchem-289	263	16	antimicrobial	antimicrobial	ADJ
eurjchem-289	263	17	activity	activity	NOUN
eurjchem-289	263	18	using	use	VERB
eurjchem-289	263	19	:	:	PUNCT
eurjchem-289	263	20	staphylococcus	staphylococcus	NOUN
eurjchem-289	263	21	aureus	aureus	NOUN
eurjchem-289	263	22	and	and	CCONJ
eurjchem-289	263	23	bacillus	bacillus	NOUN
eurjchem-289	263	24	subtilis	subtili	NOUN
eurjchem-289	263	25	(	(	PUNCT
eurjchem-289	263	26	gram	gram	NOUN
eurjchem-289	263	27	positive	positive	ADJ
eurjchem-289	263	28	bacteria	bacteria	NOUN
eurjchem-289	263	29	)	)	PUNCT
eurjchem-289	263	30	,	,	PUNCT
eurjchem-289	263	31	escherichia	escherichia	NOUN
eurjchem-289	263	32	coli	coli	NOUN
eurjchem-289	263	33	and	and	CCONJ
eurjchem-289	263	34	pseudomonas	pseudomona	NOUN
eurjchem-289	263	35	aeruginosa	aeruginosa	NOUN
eurjchem-289	263	36	(	(	PUNCT
eurjchem-289	263	37	gram	gram	NOUN
eurjchem-289	263	38	negative	negative	ADJ
eurjchem-289	263	39	bacteria	bacteria	NOUN
eurjchem-289	263	40	)	)	PUNCT
eurjchem-289	263	41	and	and	CCONJ
eurjchem-289	263	42	candida	candida	PROPN
eurjchem-289	263	43	albicans	albican	NOUN
eurjchem-289	263	44	(	(	PUNCT
eurjchem-289	263	45	fungus	fungus	NOUN
eurjchem-289	263	46	)	)	PUNCT
eurjchem-289	263	47	.	.	PUNCT
eurjchem-289	264	1	culture	culture	NOUN
eurjchem-289	264	2	media	medium	NOUN
eurjchem-289	264	3	:	:	PUNCT
eurjchem-289	264	4	nutrient	nutrient	NOUN
eurjchem-289	264	5	broth	broth	NOUN
eurjchem-289	264	6	,	,	PUNCT
eurjchem-289	264	7	sabouraud	sabouraud	NOUN
eurjchem-289	264	8	’s	’s	PART
eurjchem-289	264	9	broth	broth	NOUN
eurjchem-289	264	10	and	and	CCONJ
eurjchem-289	264	11	agar	agar	NOUN
eurjchem-289	264	12	.	.	PUNCT
eurjchem-289	265	1	2.3.2	2.3.2	NUM
eurjchem-289	265	2	.	.	X
eurjchem-289	265	3	method	method	NOUN
eurjchem-289	265	4	agar	agar	NOUN
eurjchem-289	265	5	plate	plate	NOUN
eurjchem-289	265	6	diffusion	diffusion	NOUN
eurjchem-289	265	7	technique	technique	NOUN
eurjchem-289	265	8	:	:	PUNCT
eurjchem-289	265	9	agar	agar	NOUN
eurjchem-289	265	10	plates	plate	NOUN
eurjchem-289	265	11	containing	contain	VERB
eurjchem-289	265	12	15	15	NUM
eurjchem-289	265	13	ml	ml	NOUN
eurjchem-289	265	14	of	of	ADP
eurjchem-289	265	15	agar	agar	NOUN
eurjchem-289	265	16	medium	medium	NOUN
eurjchem-289	265	17	[	[	X
eurjchem-289	265	18	nutrient	nutrient	NOUN
eurjchem-289	265	19	agar	agar	NOUN
eurjchem-289	265	20	for	for	ADP
eurjchem-289	265	21	bacteria	bacteria	NOUN
eurjchem-289	265	22	and	and	CCONJ
eurjchem-289	265	23	sabouraud	sabouraud	NOUN
eurjchem-289	265	24	’s	’s	PART
eurjchem-289	265	25	broth	broth	NOUN
eurjchem-289	265	26	for	for	ADP
eurjchem-289	265	27	fungi	fungi	PROPN
eurjchem-289	265	28	]	]	PUNCT
eurjchem-289	265	29	were	be	AUX
eurjchem-289	265	30	seeded	seed	VERB
eurjchem-289	265	31	with	with	ADP
eurjchem-289	265	32	0.2	0.2	NUM
eurjchem-289	265	33	ml	ml	NOUN
eurjchem-289	265	34	of	of	ADP
eurjchem-289	265	35	broth	broth	ADJ
eurjchem-289	265	36	culture	culture	NOUN
eurjchem-289	265	37	of	of	ADP
eurjchem-289	265	38	each	each	DET
eurjchem-289	265	39	organism	organism	NOUN
eurjchem-289	265	40	and	and	CCONJ
eurjchem-289	265	41	cultered	cultere	VERB
eurjchem-289	265	42	for	for	ADP
eurjchem-289	265	43	18	18	NUM
eurjchem-289	265	44	h.	h.	NOUN
eurjchem-289	265	45	sterile	sterile	ADJ
eurjchem-289	265	46	filter	filter	NOUN
eurjchem-289	265	47	paper	paper	NOUN
eurjchem-289	265	48	discs	disc	NOUN
eurjchem-289	265	49	(	(	PUNCT
eurjchem-289	265	50	6	6	NUM
eurjchem-289	265	51	mm	mm	NOUN
eurjchem-289	265	52	in	in	ADP
eurjchem-289	265	53	diameter	diameter	NOUN
eurjchem-289	265	54	)	)	PUNCT
eurjchem-289	265	55	were	be	AUX
eurjchem-289	265	56	impregnated	impregnate	VERB
eurjchem-289	265	57	each	each	PRON
eurjchem-289	265	58	with	with	ADP
eurjchem-289	265	59	10	10	NUM
eurjchem-289	265	60	µl	µl	NOUN
eurjchem-289	265	61	of	of	ADP
eurjchem-289	265	62	a	a	DET
eurjchem-289	265	63	1	1	NUM
eurjchem-289	265	64	%	%	NOUN
eurjchem-289	265	65	solution	solution	NOUN
eurjchem-289	265	66	of	of	ADP
eurjchem-289	265	67	the	the	DET
eurjchem-289	265	68	test	test	NOUN
eurjchem-289	265	69	compound	compound	NOUN
eurjchem-289	265	70	in	in	ADP
eurjchem-289	265	71	dmf	dmf	PROPN
eurjchem-289	265	72	and	and	CCONJ
eurjchem-289	265	73	allowed	allow	VERB
eurjchem-289	265	74	to	to	PART
eurjchem-289	265	75	air	air	VERB
eurjchem-289	265	76	dry	dry	ADJ
eurjchem-289	265	77	.	.	PUNCT
eurjchem-289	266	1	the	the	DET
eurjchem-289	266	2	discs	disc	NOUN
eurjchem-289	266	3	were	be	AUX
eurjchem-289	266	4	then	then	ADV
eurjchem-289	266	5	placed	place	VERB
eurjchem-289	266	6	onto	onto	ADP
eurjchem-289	266	7	the	the	DET
eurjchem-289	266	8	surface	surface	NOUN
eurjchem-289	266	9	of	of	ADP
eurjchem-289	266	10	agar	agar	NOUN
eurjchem-289	266	11	plates	plate	NOUN
eurjchem-289	266	12	and	and	CCONJ
eurjchem-289	266	13	incubated	incubate	VERB
eurjchem-289	266	14	at	at	ADP
eurjchem-289	266	15	37	37	NUM
eurjchem-289	266	16	oc	oc	NOUN
eurjchem-289	266	17	for	for	ADP
eurjchem-289	266	18	24	24	NUM
eurjchem-289	266	19	h.	h.	PROPN
eurjchem-289	266	20	control	control	PROPN
eurjchem-289	266	21	discs	disc	NOUN
eurjchem-289	266	22	impregnated	impregnate	VERB
eurjchem-289	266	23	with	with	ADP
eurjchem-289	266	24	dmf	dmf	PROPN
eurjchem-289	266	25	were	be	AUX
eurjchem-289	266	26	used	use	VERB
eurjchem-289	266	27	alone	alone	ADV
eurjchem-289	266	28	to	to	PART
eurjchem-289	266	29	determine	determine	VERB
eurjchem-289	266	30	the	the	DET
eurjchem-289	266	31	solvent	solvent	ADJ
eurjchem-289	266	32	activity	activity	NOUN
eurjchem-289	266	33	.	.	PUNCT
eurjchem-289	267	1	the	the	DET
eurjchem-289	267	2	antibacterial	antibacterial	ADJ
eurjchem-289	267	3	reference	reference	NOUN
eurjchem-289	267	4	tetracycline	tetracycline	NOUN
eurjchem-289	267	5	and	and	CCONJ
eurjchem-289	267	6	the	the	DET
eurjchem-289	267	7	antifungal	antifungal	ADJ
eurjchem-289	267	8	reference	reference	NOUN
eurjchem-289	267	9	nystatin	nystatin	NOUN
eurjchem-289	267	10	discs	disc	NOUN
eurjchem-289	267	11	were	be	AUX
eurjchem-289	267	12	tested	test	VERB
eurjchem-289	267	13	concurrently	concurrently	ADV
eurjchem-289	267	14	as	as	ADP
eurjchem-289	267	15	standards	standard	NOUN
eurjchem-289	267	16	.	.	PUNCT
eurjchem-289	268	1	the	the	DET
eurjchem-289	268	2	diameter	diameter	NOUN
eurjchem-289	268	3	of	of	ADP
eurjchem-289	268	4	the	the	DET
eurjchem-289	268	5	inhibition	inhibition	NOUN
eurjchem-289	268	6	zone	zone	NOUN
eurjchem-289	268	7	around	around	ADP
eurjchem-289	268	8	each	each	DET
eurjchem-289	268	9	disc	disc	NOUN
eurjchem-289	268	10	was	be	AUX
eurjchem-289	268	11	measured	measure	VERB
eurjchem-289	268	12	(	(	PUNCT
eurjchem-289	268	13	mm	mm	NOUN
eurjchem-289	268	14	)	)	PUNCT
eurjchem-289	268	15	.	.	PUNCT
eurjchem-289	269	1	2.4	2.4	NUM
eurjchem-289	269	2	.	.	PUNCT
eurjchem-289	270	1	biological	biological	ADJ
eurjchem-289	270	2	tests	test	NOUN
eurjchem-289	270	3	kinase	kinase	VERB
eurjchem-289	270	4	preparations	preparation	NOUN
eurjchem-289	270	5	and	and	CCONJ
eurjchem-289	270	6	assays	assay	NOUN
eurjchem-289	270	7	were	be	AUX
eurjchem-289	270	8	performed	perform	VERB
eurjchem-289	270	9	according	accord	VERB
eurjchem-289	270	10	to	to	ADP
eurjchem-289	270	11	the	the	DET
eurjchem-289	270	12	reported	report	VERB
eurjchem-289	270	13	procedures	procedure	NOUN
eurjchem-289	270	14	[	[	X
eurjchem-289	270	15	27‐29	27‐29	NUM
eurjchem-289	270	16	]	]	PUNCT
eurjchem-289	270	17	.	.	PUNCT
eurjchem-289	271	1	kinase	kinase	PROPN
eurjchem-289	271	2	activities	activity	NOUN
eurjchem-289	271	3	were	be	AUX
eurjchem-289	271	4	assayed	assayed	ADJ
eurjchem-289	271	5	in	in	ADP
eurjchem-289	271	6	buffer	buffer	NOUN
eurjchem-289	271	7	a	a	DET
eurjchem-289	271	8	(	(	PUNCT
eurjchem-289	271	9	10	10	NUM
eurjchem-289	271	10	mm	mm	NOUN
eurjchem-289	271	11	mgcl2	mgcl2	PROPN
eurjchem-289	271	12	,	,	PUNCT
eurjchem-289	271	13	1	1	NUM
eurjchem-289	271	14	mm	mm	NUM
eurjchem-289	271	15	egta	egta	NOUN
eurjchem-289	271	16	,	,	PUNCT
eurjchem-289	271	17	1	1	NUM
eurjchem-289	271	18	mm	mm	NUM
eurjchem-289	271	19	dtt	dtt	NOUN
eurjchem-289	271	20	,	,	PUNCT
eurjchem-289	271	21	25	25	NUM
eurjchem-289	271	22	mm	mm	PROPN
eurjchem-289	271	23	tris‐hcl	tris‐hcl	PROPN
eurjchem-289	271	24	(	(	PUNCT
eurjchem-289	271	25	ph	ph	PROPN
eurjchem-289	271	26	=	=	NOUN
eurjchem-289	271	27	7.5	7.5	NUM
eurjchem-289	271	28	)	)	PUNCT
eurjchem-289	271	29	,	,	PUNCT
eurjchem-289	271	30	50	50	NUM
eurjchem-289	271	31	µg	µg	ADV
eurjchem-289	271	32	heparin	heparin	NOUN
eurjchem-289	271	33	/	/	SYM
eurjchem-289	271	34	ml	ml	NOUN
eurjchem-289	271	35	.	.	PUNCT
eurjchem-289	271	36	)	)	PUNCT
eurjchem-289	272	1	or	or	CCONJ
eurjchem-289	272	2	c	c	X
eurjchem-289	272	3	(	(	PUNCT
eurjchem-289	272	4	60	60	NUM
eurjchem-289	272	5	mm	mm	PROPN
eurjchem-289	272	6	ß‐	ß‐	NOUN
eurjchem-289	272	7	glycerophosphate	glycerophosphate	NOUN
eurjchem-289	272	8	,	,	PUNCT
eurjchem-289	272	9	15	15	NUM
eurjchem-289	272	10	mm	mm	NOUN
eurjchem-289	272	11	p‐nitrophenylphosphate	p‐nitrophenylphosphate	NUM
eurjchem-289	272	12	,	,	PUNCT
eurjchem-289	272	13	25	25	NUM
eurjchem-289	272	14	mm	mm	NOUN
eurjchem-289	272	15	mops	mop	NOUN
eurjchem-289	272	16	(	(	PUNCT
eurjchem-289	272	17	ph	ph	NOUN
eurjchem-289	272	18	=	=	NOUN
eurjchem-289	272	19	7.2	7.2	NUM
eurjchem-289	272	20	)	)	PUNCT
eurjchem-289	272	21	,	,	PUNCT
eurjchem-289	272	22	5	5	NUM
eurjchem-289	272	23	mm	mm	NUM
eurjchem-289	272	24	egta	egta	NOUN
eurjchem-289	272	25	,	,	PUNCT
eurjchem-289	272	26	15	15	NUM
eurjchem-289	272	27	mm	mm	NOUN
eurjchem-289	272	28	mgcl2	mgcl2	PROPN
eurjchem-289	272	29	,	,	PUNCT
eurjchem-289	272	30	1	1	NUM
eurjchem-289	272	31	mm	mm	NUM
eurjchem-289	272	32	dtt	dtt	NOUN
eurjchem-289	272	33	,	,	PUNCT
eurjchem-289	272	34	1	1	NUM
eurjchem-289	272	35	mm	mm	NUM
eurjchem-289	272	36	sodium	sodium	NOUN
eurjchem-289	272	37	vanadate	vanadate	NOUN
eurjchem-289	272	38	,	,	PUNCT
eurjchem-289	272	39	1	1	NUM
eurjchem-289	272	40	mm	mm	NOUN
eurjchem-289	272	41	phenylphosphate	phenylphosphate	NOUN
eurjchem-289	272	42	)	)	PUNCT
eurjchem-289	272	43	at	at	ADP
eurjchem-289	272	44	30	30	NUM
eurjchem-289	272	45	°	°	NOUN
eurjchem-289	272	46	c	c	NOUN
eurjchem-289	272	47	,	,	PUNCT
eurjchem-289	272	48	at	at	ADP
eurjchem-289	272	49	a	a	DET
eurjchem-289	272	50	final	final	ADJ
eurjchem-289	272	51	atp	atp	NOUN
eurjchem-289	272	52	concentration	concentration	NOUN
eurjchem-289	272	53	of	of	ADP
eurjchem-289	272	54	15	15	NUM
eurjchem-289	272	55	µm	µm	NOUN
eurjchem-289	272	56	.	.	PUNCT
eurjchem-289	273	1	blank	blank	ADJ
eurjchem-289	273	2	values	value	NOUN
eurjchem-289	273	3	were	be	AUX
eurjchem-289	273	4	subtracted	subtract	VERB
eurjchem-289	273	5	and	and	CCONJ
eurjchem-289	273	6	activities	activity	NOUN
eurjchem-289	273	7	expressed	express	VERB
eurjchem-289	273	8	in	in	ADP
eurjchem-289	273	9	%	%	NOUN
eurjchem-289	273	10	of	of	ADP
eurjchem-289	273	11	the	the	DET
eurjchem-289	273	12	maximal	maximal	ADJ
eurjchem-289	273	13	activity	activity	NOUN
eurjchem-289	273	14	,	,	PUNCT
eurjchem-289	273	15	i.e.	i.e.	X
eurjchem-289	273	16	in	in	ADP
eurjchem-289	273	17	the	the	DET
eurjchem-289	273	18	absence	absence	NOUN
eurjchem-289	273	19	of	of	ADP
eurjchem-289	273	20	inhibitors	inhibitor	NOUN
eurjchem-289	273	21	.	.	PUNCT
eurjchem-289	274	1	controls	control	NOUN
eurjchem-289	274	2	were	be	AUX
eurjchem-289	274	3	performed	perform	VERB
eurjchem-289	274	4	with	with	ADP
eurjchem-289	274	5	appropriate	appropriate	ADJ
eurjchem-289	274	6	dilutions	dilution	NOUN
eurjchem-289	274	7	of	of	ADP
eurjchem-289	274	8	dmso	dmso	NOUN
eurjchem-289	274	9	.	.	PUNCT
eurjchem-289	275	1	cdk1	cdk1	PROPN
eurjchem-289	275	2	/	/	SYM
eurjchem-289	275	3	cyclin	cyclin	PROPN
eurjchem-289	275	4	b	b	PROPN
eurjchem-289	275	5	(	(	PUNCT
eurjchem-289	275	6	m	m	NOUN
eurjchem-289	275	7	phase	phase	NOUN
eurjchem-289	275	8	starfish	starfish	NOUN
eurjchem-289	275	9	oocytes	oocyte	NOUN
eurjchem-289	275	10	,	,	PUNCT
eurjchem-289	275	11	native	native	ADJ
eurjchem-289	275	12	)	)	PUNCT
eurjchem-289	275	13	,	,	PUNCT
eurjchem-289	275	14	cdk2	cdk2	PROPN
eurjchem-289	275	15	/	/	SYM
eurjchem-289	275	16	cyclin	cyclin	PROPN
eurjchem-289	275	17	a	a	PROPN
eurjchem-289	275	18	,	,	PUNCT
eurjchem-289	275	19	cdk2	cdk2	PROPN
eurjchem-289	275	20	/	/	SYM
eurjchem-289	275	21	cyclin	cyclin	PROPN
eurjchem-289	275	22	e	e	PROPN
eurjchem-289	275	23	,	,	PUNCT
eurjchem-289	275	24	cdk5	cdk5	PROPN
eurjchem-289	275	25	/	/	SYM
eurjchem-289	275	26	p25	p25	PROPN
eurjchem-289	275	27	and	and	CCONJ
eurjchem-289	275	28	cdk7	cdk7	PROPN
eurjchem-289	275	29	/	/	SYM
eurjchem-289	275	30	cyclin	cyclin	PROPN
eurjchem-289	275	31	h	h	PROPN
eurjchem-289	275	32	(	(	PUNCT
eurjchem-289	275	33	human	human	ADJ
eurjchem-289	275	34	,	,	PUNCT
eurjchem-289	275	35	recombinant	recombinant	ADJ
eurjchem-289	275	36	)	)	PUNCT
eurjchem-289	275	37	were	be	AUX
eurjchem-289	275	38	prepared	prepare	VERB
eurjchem-289	275	39	as	as	SCONJ
eurjchem-289	275	40	previously	previously	ADV
eurjchem-289	275	41	described	describe	VERB
eurjchem-289	275	42	.	.	PUNCT
eurjchem-289	276	1	their	their	PRON
eurjchem-289	276	2	kinase	kinase	NOUN
eurjchem-289	276	3	activity	activity	NOUN
eurjchem-289	276	4	was	be	AUX
eurjchem-289	276	5	assayed	assayed	ADJ
eurjchem-289	276	6	in	in	ADP
eurjchem-289	276	7	buffer	buffer	NOUN
eurjchem-289	276	8	c	c	NOUN
eurjchem-289	276	9	,	,	PUNCT
eurjchem-289	276	10	with	with	ADP
eurjchem-289	276	11	1	1	NUM
eurjchem-289	276	12	mg	mg	PROPN
eurjchem-289	276	13	histone	histone	NOUN
eurjchem-289	276	14	h1	h1	PROPN
eurjchem-289	276	15	/	/	SYM
eurjchem-289	276	16	ml	ml	PROPN
eurjchem-289	276	17	,	,	PUNCT
eurjchem-289	276	18	in	in	ADP
eurjchem-289	276	19	the	the	DET
eurjchem-289	276	20	presence	presence	NOUN
eurjchem-289	276	21	of	of	ADP
eurjchem-289	276	22	15	15	NUM
eurjchem-289	276	23	µm	µm	ADP
eurjchem-289	276	24	[	[	X
eurjchem-289	276	25	‐33p	‐33p	PROPN
eurjchem-289	276	26	]	]	X
eurjchem-289	276	27	atp	atp	PROPN
eurjchem-289	276	28	(	(	PUNCT
eurjchem-289	276	29	3,000	3,000	NUM
eurjchem-289	276	30	ci	ci	NOUN
eurjchem-289	276	31	/	/	SYM
eurjchem-289	276	32	mmol	mmol	NOUN
eurjchem-289	276	33	;	;	PUNCT
eurjchem-289	276	34	10	10	NUM
eurjchem-289	276	35	mci	mci	NOUN
eurjchem-289	276	36	/	/	SYM
eurjchem-289	276	37	ml	ml	NOUN
eurjchem-289	276	38	)	)	PUNCT
eurjchem-289	276	39	in	in	ADP
eurjchem-289	276	40	a	a	DET
eurjchem-289	276	41	final	final	ADJ
eurjchem-289	276	42	volume	volume	NOUN
eurjchem-289	276	43	of	of	ADP
eurjchem-289	276	44	30	30	NUM
eurjchem-289	276	45	µl	µl	NOUN
eurjchem-289	276	46	.	.	PUNCT
eurjchem-289	277	1	after	after	ADP
eurjchem-289	277	2	30	30	NUM
eurjchem-289	277	3	min	min	NOUN
eurjchem-289	277	4	incubation	incubation	NOUN
eurjchem-289	277	5	at	at	ADP
eurjchem-289	277	6	30	30	NUM
eurjchem-289	277	7	°	°	NOUN
eurjchem-289	277	8	c	c	NOUN
eurjchem-289	277	9	,	,	PUNCT
eurjchem-289	277	10	25	25	NUM
eurjchem-289	277	11	µl	µl	ADP
eurjchem-289	277	12	aliquots	aliquot	NOUN
eurjchem-289	277	13	of	of	ADP
eurjchem-289	277	14	supernatant	supernatant	NOUN
eurjchem-289	277	15	were	be	AUX
eurjchem-289	277	16	spotted	spot	VERB
eurjchem-289	277	17	onto	onto	ADP
eurjchem-289	277	18	2.5	2.5	NUM
eurjchem-289	277	19	x	x	SYM
eurjchem-289	277	20	3	3	NUM
eurjchem-289	277	21	cm	cm	NOUN
eurjchem-289	277	22	pieces	piece	NOUN
eurjchem-289	277	23	of	of	ADP
eurjchem-289	277	24	whatman	whatman	NOUN
eurjchem-289	277	25	p81	p81	PROPN
eurjchem-289	277	26	phosphocellulose	phosphocellulose	ADJ
eurjchem-289	277	27	paper	paper	NOUN
eurjchem-289	277	28	,	,	PUNCT
eurjchem-289	277	29	and	and	CCONJ
eurjchem-289	277	30	,	,	PUNCT
eurjchem-289	277	31	20	20	NUM
eurjchem-289	277	32	sec	sec	PROPN
eurjchem-289	277	33	later	later	ADV
eurjchem-289	277	34	,	,	PUNCT
eurjchem-289	277	35	the	the	DET
eurjchem-289	277	36	filters	filter	NOUN
eurjchem-289	277	37	were	be	AUX
eurjchem-289	277	38	washed	wash	VERB
eurjchem-289	277	39	five	five	NUM
eurjchem-289	277	40	times	time	NOUN
eurjchem-289	277	41	(	(	PUNCT
eurjchem-289	277	42	for	for	ADP
eurjchem-289	277	43	at	at	ADV
eurjchem-289	277	44	least	least	ADV
eurjchem-289	277	45	5	5	NUM
eurjchem-289	277	46	min	min	NOUN
eurjchem-289	277	47	each	each	DET
eurjchem-289	277	48	time	time	NOUN
eurjchem-289	277	49	)	)	PUNCT
eurjchem-289	277	50	in	in	ADP
eurjchem-289	277	51	a	a	DET
eurjchem-289	277	52	solution	solution	NOUN
eurjchem-289	277	53	of	of	ADP
eurjchem-289	277	54	10	10	NUM
eurjchem-289	277	55	ml	ml	ADV
eurjchem-289	277	56	phosphoric	phosphoric	ADJ
eurjchem-289	277	57	acid	acid	NOUN
eurjchem-289	277	58	/	/	SYM
eurjchem-289	277	59	liter	liter	NOUN
eurjchem-289	277	60	of	of	ADP
eurjchem-289	277	61	water	water	NOUN
eurjchem-289	277	62	.	.	PUNCT
eurjchem-289	278	1	the	the	DET
eurjchem-289	278	2	wet	wet	ADJ
eurjchem-289	278	3	filters	filter	NOUN
eurjchem-289	278	4	were	be	AUX
eurjchem-289	278	5	counted	count	VERB
eurjchem-289	278	6	in	in	ADP
eurjchem-289	278	7	the	the	DET
eurjchem-289	278	8	presence	presence	NOUN
eurjchem-289	278	9	of	of	ADP
eurjchem-289	278	10	1	1	NUM
eurjchem-289	278	11	ml	ml	NOUN
eurjchem-289	278	12	acs	acs	PROPN
eurjchem-289	278	13	(	(	PUNCT
eurjchem-289	278	14	amersham	amersham	PROPN
eurjchem-289	278	15	)	)	PUNCT
eurjchem-289	278	16	scintillation	scintillation	NOUN
eurjchem-289	278	17	fluid	fluid	NOUN
eurjchem-289	278	18	(	(	PUNCT
eurjchem-289	278	19	table	table	NOUN
eurjchem-289	278	20	1	1	NUM
eurjchem-289	278	21	)	)	PUNCT
eurjchem-289	278	22	.	.	PUNCT
eurjchem-289	279	1	gsk‐3	gsk‐3	NOUN
eurjchem-289	279	2	(	(	PUNCT
eurjchem-289	279	3	porcine	porcine	NOUN
eurjchem-289	279	4	brain	brain	NOUN
eurjchem-289	279	5	,	,	PUNCT
eurjchem-289	279	6	native	native	ADJ
eurjchem-289	279	7	)	)	PUNCT
eurjchem-289	279	8	was	be	AUX
eurjchem-289	279	9	assayed	assayed	ADJ
eurjchem-289	279	10	,	,	PUNCT
eurjchem-289	279	11	as	as	SCONJ
eurjchem-289	279	12	described	describe	VERB
eurjchem-289	279	13	for	for	ADP
eurjchem-289	279	14	cdk1	cdk1	PROPN
eurjchem-289	279	15	but	but	CCONJ
eurjchem-289	279	16	in	in	ADP
eurjchem-289	279	17	buffer	buffer	NOUN
eurjchem-289	279	18	a	a	PRON
eurjchem-289	279	19	and	and	CCONJ
eurjchem-289	279	20	using	use	VERB
eurjchem-289	279	21	a	a	DET
eurjchem-289	279	22	gsk‐3	gsk‐3	PRON
eurjchem-289	279	23	specific	specific	ADJ
eurjchem-289	279	24	substrate	substrate	NOUN
eurjchem-289	279	25	(	(	PUNCT
eurjchem-289	279	26	gs‐1	gs‐1	NOUN
eurjchem-289	279	27	:	:	PUNCT
eurjchem-289	279	28	yrraavppspslsrhssphqspedeee	yrraavppspslsrhssphqspedeee	NOUN
eurjchem-289	279	29	)	)	PUNCT
eurjchem-289	279	30	(	(	PUNCT
eurjchem-289	279	31	ps	ps	NOUN
eurjchem-289	279	32	stands	stand	VERB
eurjchem-289	279	33	for	for	ADP
eurjchem-289	279	34	phosphorylated	phosphorylate	VERB
eurjchem-289	279	35	serine	serine	NOUN
eurjchem-289	279	36	)	)	PUNCT
eurjchem-289	279	37	.	.	PUNCT
eurjchem-289	280	1	gs‐1	gs‐1	PROPN
eurjchem-289	280	2	was	be	AUX
eurjchem-289	280	3	synthesized	synthesize	VERB
eurjchem-289	280	4	by	by	ADP
eurjchem-289	280	5	millegen	millegen	PROPN
eurjchem-289	280	6	(	(	PUNCT
eurjchem-289	280	7	labege	labege	PROPN
eurjchem-289	280	8	,	,	PUNCT
eurjchem-289	280	9	france	france	PROPN
eurjchem-289	280	10	)	)	PUNCT
eurjchem-289	280	11	.	.	PUNCT
eurjchem-289	281	1	ck1	ck1	NOUN
eurjchem-289	281	2	(	(	PUNCT
eurjchem-289	281	3	porcine	porcine	NOUN
eurjchem-289	281	4	brain	brain	NOUN
eurjchem-289	281	5	,	,	PUNCT
eurjchem-289	281	6	native	native	ADJ
eurjchem-289	281	7	)	)	PUNCT
eurjchem-289	281	8	was	be	AUX
eurjchem-289	281	9	assayed	assay	VERB
eurjchem-289	281	10	as	as	SCONJ
eurjchem-289	281	11	described	describe	VERB
eurjchem-289	281	12	for	for	ADP
eurjchem-289	281	13	cdk1	cdk1	PROPN
eurjchem-289	281	14	but	but	CCONJ
eurjchem-289	281	15	using	use	VERB
eurjchem-289	281	16	the	the	DET
eurjchem-289	281	17	ck1‐specific	ck1‐specific	PROPN
eurjchem-289	281	18	peptide	peptide	NOUN
eurjchem-289	281	19	substrate	substrate	NOUN
eurjchem-289	281	20	rrkhaaigpsaysita	rrkhaaigpsaysita	NOUN
eurjchem-289	281	21	,	,	PUNCT
eurjchem-289	281	22	obtained	obtain	VERB
eurjchem-289	281	23	from	from	ADP
eurjchem-289	281	24	millegen	millegen	PROPN
eurjchem-289	281	25	(	(	PUNCT
eurjchem-289	281	26	labege	labege	PROPN
eurjchem-289	281	27	,	,	PUNCT
eurjchem-289	281	28	france	france	PROPN
eurjchem-289	281	29	)	)	PUNCT
eurjchem-289	281	30	.	.	PUNCT
eurjchem-289	282	1	3	3	X
eurjchem-289	282	2	.	.	NOUN
eurjchem-289	282	3	results	result	NOUN
eurjchem-289	282	4	and	and	CCONJ
eurjchem-289	282	5	discussion	discussion	NOUN
eurjchem-289	282	6	3.1	3.1	NUM
eurjchem-289	282	7	.	.	PUNCT
eurjchem-289	283	1	chemistry	chemistry	NOUN
eurjchem-289	283	2	the	the	DET
eurjchem-289	283	3	target	target	NOUN
eurjchem-289	283	4	compounds	compound	NOUN
eurjchem-289	283	5	were	be	AUX
eurjchem-289	283	6	prepared	prepare	VERB
eurjchem-289	283	7	according	accord	VERB
eurjchem-289	283	8	to	to	ADP
eurjchem-289	283	9	schemes	scheme	NOUN
eurjchem-289	283	10	1‐3	1‐3	PROPN
eurjchem-289	283	11	.	.	PUNCT
eurjchem-289	284	1	compound	compound	NOUN
eurjchem-289	284	2	2	2	NUM
eurjchem-289	284	3	can	can	AUX
eurjchem-289	284	4	exist	exist	VERB
eurjchem-289	284	5	in	in	ADP
eurjchem-289	284	6	two	two	NUM
eurjchem-289	284	7	tautomeric	tautomeric	ADJ
eurjchem-289	284	8	forms	form	NOUN
eurjchem-289	284	9	:	:	PUNCT
eurjchem-289	284	10	the	the	DET
eurjchem-289	284	11	imine	imine	NOUN
eurjchem-289	284	12	and	and	CCONJ
eurjchem-289	284	13	the	the	DET
eurjchem-289	284	14	enamine	enamine	NOUN
eurjchem-289	284	15	which	which	PRON
eurjchem-289	284	16	is	be	AUX
eurjchem-289	284	17	the	the	DET
eurjchem-289	284	18	more	more	ADV
eurjchem-289	284	19	predominant	predominant	ADJ
eurjchem-289	284	20	tautomer	tautomer	NOUN
eurjchem-289	284	21	[	[	X
eurjchem-289	284	22	30	30	NUM
eurjchem-289	284	23	]	]	PUNCT
eurjchem-289	284	24	.	.	PUNCT
eurjchem-289	285	1	in	in	ADP
eurjchem-289	285	2	this	this	DET
eurjchem-289	285	3	study	study	NOUN
eurjchem-289	285	4	,	,	PUNCT
eurjchem-289	285	5	our	our	PRON
eurjchem-289	285	6	target	target	NOUN
eurjchem-289	285	7	was	be	AUX
eurjchem-289	285	8	to	to	PART
eurjchem-289	285	9	synthesize	synthesize	VERB
eurjchem-289	285	10	novel	novel	ADJ
eurjchem-289	285	11	quinoxalines	quinoxaline	NOUN
eurjchem-289	285	12	through	through	ADP
eurjchem-289	285	13	the	the	DET
eurjchem-289	285	14	application	application	NOUN
eurjchem-289	285	15	of	of	ADP
eurjchem-289	285	16	aliphatic	aliphatic	ADJ
eurjchem-289	285	17	electrophilic	electrophilic	ADJ
eurjchem-289	285	18	substitution	substitution	NOUN
eurjchem-289	285	19	reactions	reaction	NOUN
eurjchem-289	285	20	on	on	ADP
eurjchem-289	285	21	the	the	DET
eurjchem-289	285	22	methyl	methyl	NOUN
eurjchem-289	285	23	and	and	CCONJ
eurjchem-289	285	24	methylene	methylene	NOUN
eurjchem-289	285	25	of	of	ADP
eurjchem-289	285	26	the	the	DET
eurjchem-289	285	27	side	side	NOUN
eurjchem-289	286	1	370	370	NUM
eurjchem-289	286	2	shabaan	shabaan	VERB
eurjchem-289	286	3	et	et	PROPN
eurjchem-289	286	4	al	al	PROPN
eurjchem-289	286	5	.	.	PUNCT
eurjchem-289	286	6	/	/	SYM
eurjchem-289	286	7	european	european	PROPN
eurjchem-289	286	8	journal	journal	PROPN
eurjchem-289	286	9	of	of	ADP
eurjchem-289	286	10	chemistry	chemistry	NOUN
eurjchem-289	286	11	2	2	NUM
eurjchem-289	286	12	(	(	PUNCT
eurjchem-289	286	13	3	3	NUM
eurjchem-289	286	14	)	)	PUNCT
eurjchem-289	286	15	(	(	PUNCT
eurjchem-289	286	16	2011	2011	NUM
eurjchem-289	286	17	)	)	PUNCT
eurjchem-289	286	18	365‐371	365‐371	NUM
eurjchem-289	286	19	chain	chain	NOUN
eurjchem-289	286	20	of	of	ADP
eurjchem-289	286	21	3‐acetonylquinoxalin‐2(1h)‐one	3‐acetonylquinoxalin‐2(1h)‐one	NUM
eurjchem-289	286	22	2	2	NUM
eurjchem-289	286	23	,	,	PUNCT
eurjchem-289	286	24	followed	follow	VERB
eurjchem-289	286	25	by	by	ADP
eurjchem-289	286	26	cyclization	cyclization	NOUN
eurjchem-289	286	27	reactions	reaction	NOUN
eurjchem-289	286	28	.	.	PUNCT
eurjchem-289	287	1	table	table	NOUN
eurjchem-289	287	2	1	1	NUM
eurjchem-289	287	3	.	.	PUNCT
eurjchem-289	287	4	inhibition	inhibition	NOUN
eurjchem-289	287	5	effect	effect	NOUN
eurjchem-289	287	6	(	(	PUNCT
eurjchem-289	287	7	µm	µm	NOUN
eurjchem-289	287	8	)	)	PUNCT
eurjchem-289	287	9	on	on	ADP
eurjchem-289	287	10	ck1	ck1	PROPN
eurjchem-289	287	11	,	,	PUNCT
eurjchem-289	287	12	cdk5	cdk5	NOUN
eurjchem-289	287	13	and	and	CCONJ
eurjchem-289	287	14	gsk3β	gsk3β	PROPN
eurjchem-289	287	15	of	of	ADP
eurjchem-289	287	16	selected	select	VERB
eurjchem-289	287	17	compounds	compound	NOUN
eurjchem-289	287	18	.	.	PUNCT
eurjchem-289	288	1	compound	compound	NOUN
eurjchem-289	288	2	ck1	ck1	PROPN
eurjchem-289	288	3	cdk5	cdk5	PROPN
eurjchem-289	288	4	gsk‐3β	gsk‐3β	PROPN
eurjchem-289	288	5	compound	compound	PROPN
eurjchem-289	288	6	3a	3a	PROPN
eurjchem-289	288	7	>	>	X
eurjchem-289	288	8	10	10	NUM
eurjchem-289	288	9	>	>	SYM
eurjchem-289	288	10	10	10	NUM
eurjchem-289	288	11	>	>	SYM
eurjchem-289	288	12	10	10	NUM
eurjchem-289	288	13	compound	compound	NOUN
eurjchem-289	288	14	3b	3b	NOUN
eurjchem-289	288	15	>	>	X
eurjchem-289	288	16	10	10	NUM
eurjchem-289	288	17	>	>	SYM
eurjchem-289	288	18	10	10	NUM
eurjchem-289	288	19	>	>	SYM
eurjchem-289	288	20	10	10	NUM
eurjchem-289	288	21	compound	compound	NOUN
eurjchem-289	288	22	3c	3c	NUM
eurjchem-289	288	23	>	>	PUNCT
eurjchem-289	288	24	10	10	NUM
eurjchem-289	288	25	>	>	SYM
eurjchem-289	288	26	10	10	NUM
eurjchem-289	288	27	>	>	SYM
eurjchem-289	288	28	10	10	NUM
eurjchem-289	288	29	compound	compound	NOUN
eurjchem-289	288	30	5a	5a	NUM
eurjchem-289	288	31	>	>	X
eurjchem-289	288	32	10	10	NUM
eurjchem-289	288	33	>	>	SYM
eurjchem-289	288	34	10	10	NUM
eurjchem-289	288	35	>	>	SYM
eurjchem-289	288	36	10	10	NUM
eurjchem-289	288	37	compound	compound	NOUN
eurjchem-289	288	38	5b	5b	NOUN
eurjchem-289	288	39	>	>	PUNCT
eurjchem-289	288	40	10	10	NUM
eurjchem-289	288	41	>	>	SYM
eurjchem-289	288	42	10	10	NUM
eurjchem-289	288	43	>	>	SYM
eurjchem-289	288	44	10	10	NUM
eurjchem-289	288	45	compound	compound	NOUN
eurjchem-289	288	46	6a	6a	NOUN
eurjchem-289	288	47	>	>	X
eurjchem-289	288	48	10	10	NUM
eurjchem-289	288	49	>	>	SYM
eurjchem-289	288	50	10	10	NUM
eurjchem-289	288	51	>	>	SYM
eurjchem-289	288	52	10	10	NUM
eurjchem-289	288	53	compound	compound	NOUN
eurjchem-289	288	54	6b	6b	NOUN
eurjchem-289	288	55	>	>	X
eurjchem-289	288	56	10	10	NUM
eurjchem-289	288	57	>	>	SYM
eurjchem-289	288	58	10	10	NUM
eurjchem-289	288	59	>	>	SYM
eurjchem-289	288	60	10	10	NUM
eurjchem-289	288	61	compound	compound	NOUN
eurjchem-289	288	62	6c	6c	NOUN
eurjchem-289	288	63	>	>	X
eurjchem-289	288	64	10	10	NUM
eurjchem-289	288	65	>	>	SYM
eurjchem-289	288	66	10	10	NUM
eurjchem-289	288	67	>	>	SYM
eurjchem-289	288	68	10	10	NUM
eurjchem-289	288	69	compound	compound	NOUN
eurjchem-289	288	70	7	7	NUM
eurjchem-289	288	71	>	>	X
eurjchem-289	288	72	10	10	NUM
eurjchem-289	288	73	>	>	SYM
eurjchem-289	288	74	10	10	NUM
eurjchem-289	288	75	>	>	SYM
eurjchem-289	288	76	10	10	NUM
eurjchem-289	288	77	compound	compound	NOUN
eurjchem-289	288	78	8	8	NUM
eurjchem-289	288	79	>	>	X
eurjchem-289	288	80	10	10	NUM
eurjchem-289	288	81	>	>	SYM
eurjchem-289	288	82	10	10	NUM
eurjchem-289	288	83	>	>	SYM
eurjchem-289	288	84	10	10	NUM
eurjchem-289	288	85	compound	compound	NOUN
eurjchem-289	288	86	9a	9a	NOUN
eurjchem-289	288	87	>	>	X
eurjchem-289	288	88	10	10	NUM
eurjchem-289	288	89	>	>	SYM
eurjchem-289	288	90	10	10	NUM
eurjchem-289	288	91	>	>	SYM
eurjchem-289	288	92	10	10	NUM
eurjchem-289	288	93	compound	compound	NOUN
eurjchem-289	288	94	9b	9b	NOUN
eurjchem-289	288	95	>	>	PUNCT
eurjchem-289	288	96	10	10	NUM
eurjchem-289	288	97	>	>	SYM
eurjchem-289	288	98	10	10	NUM
eurjchem-289	288	99	>	>	SYM
eurjchem-289	288	100	10	10	NUM
eurjchem-289	288	101	compound	compound	NOUN
eurjchem-289	288	102	10a	10a	NOUN
eurjchem-289	288	103	>	>	X
eurjchem-289	288	104	10	10	NUM
eurjchem-289	288	105	>	>	SYM
eurjchem-289	288	106	10	10	NUM
eurjchem-289	288	107	>	>	SYM
eurjchem-289	288	108	10	10	NUM
eurjchem-289	288	109	compound	compound	NOUN
eurjchem-289	288	110	10b	10b	NOUN
eurjchem-289	288	111	>	>	X
eurjchem-289	288	112	10	10	NUM
eurjchem-289	288	113	>	>	SYM
eurjchem-289	288	114	10	10	NUM
eurjchem-289	288	115	>	>	SYM
eurjchem-289	288	116	10	10	NUM
eurjchem-289	288	117	compound	compound	NOUN
eurjchem-289	288	118	11a	11a	NOUN
eurjchem-289	288	119	>	>	X
eurjchem-289	288	120	10	10	NUM
eurjchem-289	288	121	>	>	SYM
eurjchem-289	288	122	10	10	NUM
eurjchem-289	288	123	>	>	SYM
eurjchem-289	288	124	10	10	NUM
eurjchem-289	288	125	compound	compound	NOUN
eurjchem-289	288	126	11b	11b	NOUN
eurjchem-289	288	127	>	>	X
eurjchem-289	288	128	10	10	NUM
eurjchem-289	288	129	>	>	SYM
eurjchem-289	288	130	10	10	NUM
eurjchem-289	288	131	>	>	SYM
eurjchem-289	288	132	10	10	NUM
eurjchem-289	288	133	compound	compound	NOUN
eurjchem-289	288	134	12	12	NUM
eurjchem-289	288	135	>	>	SYM
eurjchem-289	288	136	10	10	NUM
eurjchem-289	288	137	>	>	SYM
eurjchem-289	288	138	10	10	NUM
eurjchem-289	288	139	>	>	SYM
eurjchem-289	288	140	10	10	NUM
eurjchem-289	288	141	compound	compound	NOUN
eurjchem-289	288	142	13	13	NUM
eurjchem-289	288	143	>	>	SYM
eurjchem-289	288	144	10	10	NUM
eurjchem-289	288	145	>	>	SYM
eurjchem-289	288	146	10	10	NUM
eurjchem-289	288	147	>	>	SYM
eurjchem-289	288	148	10	10	NUM
eurjchem-289	288	149	compound	compound	NOUN
eurjchem-289	288	150	14a	14a	NOUN
eurjchem-289	288	151	>	>	X
eurjchem-289	288	152	10	10	NUM
eurjchem-289	288	153	>	>	SYM
eurjchem-289	288	154	10	10	NUM
eurjchem-289	288	155	>	>	SYM
eurjchem-289	288	156	10	10	NUM
eurjchem-289	288	157	in	in	ADP
eurjchem-289	288	158	scheme	scheme	NOUN
eurjchem-289	288	159	1	1	NUM
eurjchem-289	288	160	,	,	PUNCT
eurjchem-289	288	161	the	the	DET
eurjchem-289	288	162	formation	formation	NOUN
eurjchem-289	288	163	of	of	ADP
eurjchem-289	288	164	chalcone	chalcone	NOUN
eurjchem-289	288	165	product	product	NOUN
eurjchem-289	288	166	was	be	AUX
eurjchem-289	288	167	catalyzed	catalyze	VERB
eurjchem-289	288	168	by	by	ADP
eurjchem-289	288	169	a	a	DET
eurjchem-289	288	170	basic	basic	ADJ
eurjchem-289	288	171	or	or	CCONJ
eurjchem-289	288	172	acidic	acidic	ADJ
eurjchem-289	288	173	catalyst	catalyst	NOUN
eurjchem-289	288	174	[	[	X
eurjchem-289	288	175	31	31	NUM
eurjchem-289	288	176	]	]	PUNCT
eurjchem-289	288	177	.	.	PUNCT
eurjchem-289	289	1	in	in	ADP
eurjchem-289	289	2	alcoholic	alcoholic	PROPN
eurjchem-289	289	3	alkali	alkali	ADJ
eurjchem-289	289	4	medium	medium	NOUN
eurjchem-289	289	5	the	the	DET
eurjchem-289	289	6	electrophilic	electrophilic	ADJ
eurjchem-289	289	7	substitution	substitution	NOUN
eurjchem-289	289	8	reaction	reaction	NOUN
eurjchem-289	289	9	occurred	occur	VERB
eurjchem-289	289	10	on	on	ADP
eurjchem-289	289	11	the	the	DET
eurjchem-289	289	12	terminal	terminal	ADJ
eurjchem-289	289	13	methyl	methyl	NOUN
eurjchem-289	289	14	group	group	NOUN
eurjchem-289	289	15	.	.	PUNCT
eurjchem-289	290	1	1h	1h	NUM
eurjchem-289	290	2	nmr	nmr	NOUN
eurjchem-289	290	3	spectrum	spectrum	NOUN
eurjchem-289	290	4	of	of	ADP
eurjchem-289	290	5	compound	compound	NOUN
eurjchem-289	290	6	3	3	NUM
eurjchem-289	290	7	revealed	reveal	VERB
eurjchem-289	290	8	the	the	DET
eurjchem-289	290	9	disappearance	disappearance	NOUN
eurjchem-289	290	10	of	of	ADP
eurjchem-289	290	11	the	the	DET
eurjchem-289	290	12	singlet	singlet	NOUN
eurjchem-289	290	13	signal	signal	NOUN
eurjchem-289	290	14	at	at	ADP
eurjchem-289	290	15	δ	δ	PROPN
eurjchem-289	290	16	2.17	2.17	NUM
eurjchem-289	290	17	ppm	ppm	NOUN
eurjchem-289	290	18	corresponding	correspond	VERB
eurjchem-289	290	19	to	to	ADP
eurjchem-289	290	20	the	the	DET
eurjchem-289	290	21	terminal	terminal	ADJ
eurjchem-289	290	22	methyl	methyl	NOUN
eurjchem-289	290	23	protons	proton	NOUN
eurjchem-289	290	24	and	and	CCONJ
eurjchem-289	290	25	the	the	DET
eurjchem-289	290	26	presence	presence	NOUN
eurjchem-289	290	27	of	of	ADP
eurjchem-289	290	28	a	a	DET
eurjchem-289	290	29	singlet	singlet	ADJ
eurjchem-289	290	30	signal	signal	NOUN
eurjchem-289	290	31	at	at	ADP
eurjchem-289	290	32	δ	δ	PROPN
eurjchem-289	290	33	6.38	6.38	NUM
eurjchem-289	290	34	ppm	ppm	NOUN
eurjchem-289	290	35	corresponding	correspond	VERB
eurjchem-289	290	36	to	to	ADP
eurjchem-289	290	37	the	the	DET
eurjchem-289	290	38	vinylic	vinylic	ADJ
eurjchem-289	290	39	protons	proton	NOUN
eurjchem-289	290	40	.	.	PUNCT
eurjchem-289	291	1	on	on	ADP
eurjchem-289	291	2	the	the	DET
eurjchem-289	291	3	other	other	ADJ
eurjchem-289	291	4	hand	hand	NOUN
eurjchem-289	291	5	,	,	PUNCT
eurjchem-289	291	6	reaction	reaction	NOUN
eurjchem-289	291	7	in	in	ADP
eurjchem-289	291	8	acetic	acetic	ADJ
eurjchem-289	291	9	acid	acid	NOUN
eurjchem-289	291	10	afforded	afford	VERB
eurjchem-289	291	11	compound	compound	NOUN
eurjchem-289	291	12	4	4	NUM
eurjchem-289	291	13	and	and	CCONJ
eurjchem-289	291	14	its	its	PRON
eurjchem-289	291	15	1h	1h	NUM
eurjchem-289	291	16	nmr	nmr	NOUN
eurjchem-289	291	17	spectrum	spectrum	NOUN
eurjchem-289	291	18	showed	show	VERB
eurjchem-289	291	19	a	a	DET
eurjchem-289	291	20	multiplet	multiplet	NOUN
eurjchem-289	291	21	signal	signal	NOUN
eurjchem-289	291	22	at	at	ADP
eurjchem-289	291	23	δ	δ	PROPN
eurjchem-289	291	24	6.94‐7.58	6.94‐7.58	NUM
eurjchem-289	291	25	ppm	ppm	NOUN
eurjchem-289	291	26	corresponding	correspond	VERB
eurjchem-289	291	27	to	to	ADP
eurjchem-289	291	28	the	the	DET
eurjchem-289	291	29	aromatic	aromatic	ADJ
eurjchem-289	291	30	protons	proton	NOUN
eurjchem-289	291	31	and	and	CCONJ
eurjchem-289	291	32	the	the	DET
eurjchem-289	291	33	disappearance	disappearance	NOUN
eurjchem-289	291	34	of	of	ADP
eurjchem-289	291	35	both	both	DET
eurjchem-289	291	36	aliphatic	aliphatic	ADJ
eurjchem-289	291	37	protons	proton	NOUN
eurjchem-289	291	38	at	at	ADP
eurjchem-289	291	39	δ	δ	PROPN
eurjchem-289	291	40	2.17	2.17	NUM
eurjchem-289	291	41	ppm	ppm	NOUN
eurjchem-289	291	42	and	and	CCONJ
eurjchem-289	291	43	the	the	DET
eurjchem-289	291	44	vinylic	vinylic	ADJ
eurjchem-289	291	45	proton	proton	NOUN
eurjchem-289	291	46	at	at	ADP
eurjchem-289	291	47	δ	δ	PROPN
eurjchem-289	291	48	6.01	6.01	NUM
eurjchem-289	291	49	ppm	ppm	NOUN
eurjchem-289	291	50	.	.	PUNCT
eurjchem-289	292	1	mass	mass	NOUN
eurjchem-289	292	2	spectrum	spectrum	NOUN
eurjchem-289	292	3	of	of	ADP
eurjchem-289	292	4	the	the	DET
eurjchem-289	292	5	product	product	NOUN
eurjchem-289	292	6	showed	show	VERB
eurjchem-289	292	7	a	a	DET
eurjchem-289	292	8	molecular	molecular	ADJ
eurjchem-289	292	9	ion	ion	NOUN
eurjchem-289	292	10	peak	peak	NOUN
eurjchem-289	292	11	at	at	ADP
eurjchem-289	292	12	m	m	PROPN
eurjchem-289	292	13	/	/	SYM
eurjchem-289	292	14	z	z	PROPN
eurjchem-289	292	15	288	288	NUM
eurjchem-289	292	16	.	.	PUNCT
eurjchem-289	293	1	compound	compound	NOUN
eurjchem-289	293	2	4	4	NUM
eurjchem-289	293	3	was	be	AUX
eurjchem-289	293	4	prepared	prepare	VERB
eurjchem-289	293	5	by	by	ADP
eurjchem-289	293	6	two	two	NUM
eurjchem-289	293	7	different	different	ADJ
eurjchem-289	293	8	ways	way	NOUN
eurjchem-289	293	9	,	,	PUNCT
eurjchem-289	293	10	firstly	firstly	ADV
eurjchem-289	293	11	by	by	ADP
eurjchem-289	293	12	refluxing	refluxing	NOUN
eurjchem-289	293	13	of	of	ADP
eurjchem-289	293	14	compound	compound	NOUN
eurjchem-289	293	15	2	2	NUM
eurjchem-289	293	16	with	with	ADP
eurjchem-289	293	17	benzaldehyde	benzaldehyde	NOUN
eurjchem-289	293	18	in	in	ADP
eurjchem-289	293	19	glacial	glacial	ADJ
eurjchem-289	293	20	acetic	acetic	ADJ
eurjchem-289	293	21	acid	acid	NOUN
eurjchem-289	293	22	or	or	CCONJ
eurjchem-289	293	23	fusing	fuse	VERB
eurjchem-289	293	24	the	the	DET
eurjchem-289	293	25	starting	starting	NOUN
eurjchem-289	293	26	compound	compound	NOUN
eurjchem-289	293	27	2	2	NUM
eurjchem-289	293	28	with	with	ADP
eurjchem-289	293	29	benzaldehyde	benzaldehyde	NOUN
eurjchem-289	293	30	at	at	ADP
eurjchem-289	293	31	180‐190	180‐190	PROPN
eurjchem-289	293	32	oc	oc	NOUN
eurjchem-289	293	33	.	.	PUNCT
eurjchem-289	294	1	furthermore	furthermore	ADV
eurjchem-289	294	2	,	,	PUNCT
eurjchem-289	294	3	refluxing	refluxing	NOUN
eurjchem-289	294	4	of	of	ADP
eurjchem-289	294	5	compound	compound	NOUN
eurjchem-289	294	6	3a	3a	NUM
eurjchem-289	294	7	in	in	ADP
eurjchem-289	294	8	bromine	bromine	NOUN
eurjchem-289	294	9	/	/	SYM
eurjchem-289	294	10	acetic	acetic	ADJ
eurjchem-289	294	11	acid	acid	NOUN
eurjchem-289	294	12	afforded	afford	VERB
eurjchem-289	294	13	compound	compound	NOUN
eurjchem-289	294	14	4	4	NUM
eurjchem-289	294	15	.	.	PUNCT
eurjchem-289	295	1	secondly	secondly	ADV
eurjchem-289	295	2	,	,	PUNCT
eurjchem-289	295	3	hantzsch	hantzsch	ADJ
eurjchem-289	295	4	reaction	reaction	NOUN
eurjchem-289	295	5	was	be	AUX
eurjchem-289	295	6	applied	apply	VERB
eurjchem-289	295	7	on	on	ADP
eurjchem-289	295	8	2	2	NUM
eurjchem-289	295	9	using	use	VERB
eurjchem-289	295	10	ethyl	ethyl	PROPN
eurjchem-289	295	11	cyanoacetate	cyanoacetate	NOUN
eurjchem-289	295	12	in	in	ADP
eurjchem-289	295	13	ethanol	ethanol	NOUN
eurjchem-289	295	14	or	or	CCONJ
eurjchem-289	295	15	n‐butanol	n‐butanol	ADV
eurjchem-289	295	16	resulted	result	VERB
eurjchem-289	295	17	in	in	ADP
eurjchem-289	295	18	the	the	DET
eurjchem-289	295	19	same	same	ADJ
eurjchem-289	295	20	product	product	NOUN
eurjchem-289	295	21	5a	5a	NUM
eurjchem-289	295	22	in	in	ADP
eurjchem-289	295	23	yields	yield	NOUN
eurjchem-289	295	24	of	of	ADP
eurjchem-289	295	25	68	68	NUM
eurjchem-289	295	26	%	%	NOUN
eurjchem-289	295	27	and	and	CCONJ
eurjchem-289	295	28	77	77	NUM
eurjchem-289	295	29	%	%	NOUN
eurjchem-289	295	30	,	,	PUNCT
eurjchem-289	295	31	respectively	respectively	ADV
eurjchem-289	295	32	.	.	PUNCT
eurjchem-289	296	1	the	the	DET
eurjchem-289	296	2	reaction	reaction	NOUN
eurjchem-289	296	3	mechanism	mechanism	NOUN
eurjchem-289	296	4	as	as	SCONJ
eurjchem-289	296	5	guided	guide	VERB
eurjchem-289	296	6	by	by	ADP
eurjchem-289	296	7	katritzky	katritzky	PROPN
eurjchem-289	296	8	[	[	X
eurjchem-289	296	9	32	32	NUM
eurjchem-289	296	10	]	]	PUNCT
eurjchem-289	296	11	may	may	AUX
eurjchem-289	296	12	proceed	proceed	VERB
eurjchem-289	296	13	via	via	ADP
eurjchem-289	296	14	the	the	DET
eurjchem-289	296	15	formation	formation	NOUN
eurjchem-289	296	16	of	of	ADP
eurjchem-289	296	17	the	the	DET
eurjchem-289	296	18	enaminone	enaminone	NOUN
eurjchem-289	296	19	intermediate	intermediate	ADJ
eurjchem-289	296	20	.	.	PUNCT
eurjchem-289	297	1	the	the	DET
eurjchem-289	297	2	second	second	ADJ
eurjchem-289	297	3	step	step	NOUN
eurjchem-289	297	4	involved	involve	VERB
eurjchem-289	297	5	micheal	micheal	NOUN
eurjchem-289	297	6	addition	addition	NOUN
eurjchem-289	297	7	of	of	ADP
eurjchem-289	297	8	this	this	DET
eurjchem-289	297	9	intermediate	intermediate	ADJ
eurjchem-289	297	10	to	to	ADP
eurjchem-289	297	11	the	the	DET
eurjchem-289	297	12	α	α	NOUN
eurjchem-289	297	13	,	,	PUNCT
eurjchem-289	297	14	β‐	β‐	ADJ
eurjchem-289	297	15	unsaturated	unsaturate	VERB
eurjchem-289	297	16	ester	ester	NOUN
eurjchem-289	297	17	,	,	PUNCT
eurjchem-289	297	18	initially	initially	ADV
eurjchem-289	297	19	formed	form	VERB
eurjchem-289	297	20	from	from	ADP
eurjchem-289	297	21	the	the	DET
eurjchem-289	297	22	reaction	reaction	NOUN
eurjchem-289	297	23	of	of	ADP
eurjchem-289	297	24	the	the	DET
eurjchem-289	297	25	appropriate	appropriate	ADJ
eurjchem-289	297	26	aldehyde	aldehyde	NOUN
eurjchem-289	297	27	with	with	ADP
eurjchem-289	297	28	ethyl	ethyl	PROPN
eurjchem-289	297	29	cyanoacetate	cyanoacetate	NOUN
eurjchem-289	297	30	,	,	PUNCT
eurjchem-289	297	31	followed	follow	VERB
eurjchem-289	297	32	by	by	ADP
eurjchem-289	297	33	cyclization	cyclization	NOUN
eurjchem-289	297	34	and	and	CCONJ
eurjchem-289	297	35	aromatization	aromatization	NOUN
eurjchem-289	297	36	to	to	PART
eurjchem-289	297	37	yield	yield	VERB
eurjchem-289	297	38	the	the	DET
eurjchem-289	297	39	target	target	NOUN
eurjchem-289	297	40	compounds	compound	VERB
eurjchem-289	297	41	5a	5a	NUM
eurjchem-289	297	42	,	,	PUNCT
eurjchem-289	297	43	b.	b.	NOUN
eurjchem-289	297	44	on	on	ADP
eurjchem-289	297	45	the	the	DET
eurjchem-289	297	46	other	other	ADJ
eurjchem-289	297	47	hand	hand	NOUN
eurjchem-289	297	48	,	,	PUNCT
eurjchem-289	297	49	the	the	DET
eurjchem-289	297	50	reaction	reaction	NOUN
eurjchem-289	297	51	of	of	ADP
eurjchem-289	297	52	compound	compound	NOUN
eurjchem-289	297	53	2	2	NUM
eurjchem-289	297	54	with	with	ADP
eurjchem-289	297	55	aromatic	aromatic	ADJ
eurjchem-289	297	56	aldehydes	aldehyde	NOUN
eurjchem-289	297	57	,	,	PUNCT
eurjchem-289	297	58	malononitrile	malononitrile	NOUN
eurjchem-289	297	59	and	and	CCONJ
eurjchem-289	297	60	ammonium	ammonium	NOUN
eurjchem-289	297	61	acetate	acetate	NOUN
eurjchem-289	297	62	in	in	ADP
eurjchem-289	297	63	ethanol	ethanol	NOUN
eurjchem-289	297	64	gave	give	VERB
eurjchem-289	297	65	the	the	DET
eurjchem-289	297	66	products	product	NOUN
eurjchem-289	297	67	6a‐c	6a‐c	NOUN
eurjchem-289	297	68	.	.	PUNCT
eurjchem-289	298	1	moreover	moreover	ADV
eurjchem-289	298	2	,	,	PUNCT
eurjchem-289	298	3	heating	heating	NOUN
eurjchem-289	298	4	compound	compound	NOUN
eurjchem-289	298	5	2	2	NUM
eurjchem-289	298	6	with	with	ADP
eurjchem-289	298	7	paraformaldehyde	paraformaldehyde	NOUN
eurjchem-289	298	8	in	in	ADP
eurjchem-289	298	9	ethanol	ethanol	NOUN
eurjchem-289	298	10	containing	contain	VERB
eurjchem-289	298	11	acetic	acetic	ADJ
eurjchem-289	298	12	acid	acid	NOUN
eurjchem-289	298	13	yielded	yield	VERB
eurjchem-289	298	14	product	product	NOUN
eurjchem-289	298	15	7	7	NUM
eurjchem-289	298	16	[	[	SYM
eurjchem-289	298	17	33	33	NUM
eurjchem-289	298	18	]	]	PUNCT
eurjchem-289	298	19	.	.	PUNCT
eurjchem-289	299	1	1h	1h	NUM
eurjchem-289	299	2	nmr	nmr	NOUN
eurjchem-289	299	3	spectrum	spectrum	NOUN
eurjchem-289	299	4	of	of	ADP
eurjchem-289	299	5	compound	compound	NOUN
eurjchem-289	299	6	7	7	NUM
eurjchem-289	299	7	showed	show	VERB
eurjchem-289	299	8	a	a	DET
eurjchem-289	299	9	singlet	singlet	ADJ
eurjchem-289	299	10	signal	signal	NOUN
eurjchem-289	299	11	at	at	ADP
eurjchem-289	299	12	δ	δ	PROPN
eurjchem-289	299	13	2.24	2.24	NUM
eurjchem-289	299	14	ppm	ppm	NOUN
eurjchem-289	299	15	corresponding	correspond	VERB
eurjchem-289	299	16	to	to	ADP
eurjchem-289	299	17	the	the	DET
eurjchem-289	299	18	terminal	terminal	ADJ
eurjchem-289	299	19	methyl	methyl	NOUN
eurjchem-289	299	20	protons	proton	NOUN
eurjchem-289	299	21	and	and	CCONJ
eurjchem-289	299	22	the	the	DET
eurjchem-289	299	23	absence	absence	NOUN
eurjchem-289	299	24	of	of	ADP
eurjchem-289	299	25	the	the	DET
eurjchem-289	299	26	vinylic	vinylic	ADJ
eurjchem-289	299	27	proton	proton	NOUN
eurjchem-289	299	28	.	.	PUNCT
eurjchem-289	300	1	aminomethylation	aminomethylation	NOUN
eurjchem-289	300	2	of	of	ADP
eurjchem-289	300	3	compound	compound	NOUN
eurjchem-289	300	4	2	2	NUM
eurjchem-289	300	5	was	be	AUX
eurjchem-289	300	6	carried	carry	VERB
eurjchem-289	300	7	out	out	ADP
eurjchem-289	300	8	using	use	VERB
eurjchem-289	300	9	paraformaldehyde	paraformaldehyde	NOUN
eurjchem-289	300	10	and	and	CCONJ
eurjchem-289	300	11	piperidine	piperidine	NOUN
eurjchem-289	300	12	in	in	ADP
eurjchem-289	300	13	ethanol	ethanol	NOUN
eurjchem-289	300	14	containing	contain	VERB
eurjchem-289	300	15	few	few	ADJ
eurjchem-289	300	16	drops	drop	NOUN
eurjchem-289	300	17	of	of	ADP
eurjchem-289	300	18	acetic	acetic	ADJ
eurjchem-289	300	19	acid	acid	NOUN
eurjchem-289	300	20	gave	give	VERB
eurjchem-289	300	21	product	product	NOUN
eurjchem-289	300	22	8	8	NUM
eurjchem-289	300	23	.	.	PUNCT
eurjchem-289	301	1	the	the	DET
eurjchem-289	301	2	structure	structure	NOUN
eurjchem-289	301	3	assignment	assignment	NOUN
eurjchem-289	301	4	depends	depend	VERB
eurjchem-289	301	5	on	on	ADP
eurjchem-289	301	6	the	the	DET
eurjchem-289	301	7	position	position	NOUN
eurjchem-289	301	8	at	at	ADP
eurjchem-289	301	9	which	which	PRON
eurjchem-289	301	10	the	the	DET
eurjchem-289	301	11	electrophilic	electrophilic	ADJ
eurjchem-289	301	12	substitution	substitution	NOUN
eurjchem-289	301	13	reaction	reaction	NOUN
eurjchem-289	301	14	took	take	VERB
eurjchem-289	301	15	place	place	NOUN
eurjchem-289	301	16	.	.	PUNCT
eurjchem-289	302	1	ir	ir	PROPN
eurjchem-289	302	2	spectra	spectra	PROPN
eurjchem-289	302	3	showed	show	VERB
eurjchem-289	302	4	bands	band	NOUN
eurjchem-289	302	5	at	at	ADP
eurjchem-289	302	6	1375	1375	NUM
eurjchem-289	302	7	and	and	CCONJ
eurjchem-289	302	8	1380	1380	NUM
eurjchem-289	302	9	cm‐1	cm‐1	NOUN
eurjchem-289	302	10	,	,	PUNCT
eurjchem-289	302	11	respectively	respectively	ADV
eurjchem-289	302	12	,	,	PUNCT
eurjchem-289	302	13	corresponding	correspond	VERB
eurjchem-289	302	14	to	to	ADP
eurjchem-289	302	15	the	the	DET
eurjchem-289	302	16	bending	bend	VERB
eurjchem-289	302	17	vibration	vibration	NOUN
eurjchem-289	302	18	of	of	ADP
eurjchem-289	302	19	the	the	DET
eurjchem-289	302	20	terminal	terminal	ADJ
eurjchem-289	302	21	methyl	methyl	NOUN
eurjchem-289	302	22	group	group	NOUN
eurjchem-289	302	23	[	[	X
eurjchem-289	302	24	34	34	NUM
eurjchem-289	302	25	]	]	PUNCT
eurjchem-289	302	26	in	in	ADP
eurjchem-289	302	27	addition	addition	NOUN
eurjchem-289	302	28	to	to	ADP
eurjchem-289	302	29	bands	band	NOUN
eurjchem-289	302	30	at	at	ADP
eurjchem-289	302	31	3450	3450	NUM
eurjchem-289	302	32	and	and	CCONJ
eurjchem-289	302	33	3400	3400	NUM
eurjchem-289	302	34	cm‐1	cm‐1	NOUN
eurjchem-289	302	35	,	,	PUNCT
eurjchem-289	302	36	respectively	respectively	ADV
eurjchem-289	302	37	,	,	PUNCT
eurjchem-289	302	38	due	due	ADP
eurjchem-289	302	39	to	to	ADP
eurjchem-289	302	40	nh	nh	PROPN
eurjchem-289	302	41	group	group	NOUN
eurjchem-289	302	42	and	and	CCONJ
eurjchem-289	302	43	bands	band	NOUN
eurjchem-289	302	44	at	at	ADP
eurjchem-289	302	45	1690‐1650	1690‐1650	NUM
eurjchem-289	302	46	cm‐1	cm‐1	NOUN
eurjchem-289	302	47	due	due	ADP
eurjchem-289	302	48	to	to	ADP
eurjchem-289	302	49	c	c	NOUN
eurjchem-289	302	50	=	=	NOUN
eurjchem-289	302	51	o	o	NOUN
eurjchem-289	302	52	groups	group	NOUN
eurjchem-289	302	53	.	.	PUNCT
eurjchem-289	303	1	1h	1h	NUM
eurjchem-289	303	2	nmr	nmr	NOUN
eurjchem-289	303	3	spectrum	spectrum	NOUN
eurjchem-289	303	4	showed	show	VERB
eurjchem-289	303	5	a	a	DET
eurjchem-289	303	6	singlet	singlet	ADJ
eurjchem-289	303	7	signal	signal	NOUN
eurjchem-289	303	8	at	at	ADP
eurjchem-289	303	9	δ	δ	PROPN
eurjchem-289	303	10	2.38	2.38	NUM
eurjchem-289	303	11	ppm	ppm	NOUN
eurjchem-289	303	12	corresponding	correspond	VERB
eurjchem-289	303	13	to	to	ADP
eurjchem-289	303	14	the	the	DET
eurjchem-289	303	15	terminal	terminal	ADJ
eurjchem-289	303	16	methyl	methyl	NOUN
eurjchem-289	303	17	group	group	NOUN
eurjchem-289	303	18	protons	proton	NOUN
eurjchem-289	303	19	and	and	CCONJ
eurjchem-289	303	20	the	the	DET
eurjchem-289	303	21	absence	absence	NOUN
eurjchem-289	303	22	of	of	ADP
eurjchem-289	303	23	the	the	DET
eurjchem-289	303	24	vinylic	vinylic	ADJ
eurjchem-289	303	25	proton	proton	NOUN
eurjchem-289	303	26	.	.	PUNCT
eurjchem-289	304	1	dehydration	dehydration	NOUN
eurjchem-289	304	2	of	of	ADP
eurjchem-289	304	3	compounds	compound	NOUN
eurjchem-289	304	4	3a	3a	NUM
eurjchem-289	304	5	,	,	PUNCT
eurjchem-289	304	6	b	b	NOUN
eurjchem-289	304	7	in	in	ADP
eurjchem-289	304	8	acetic	acetic	ADJ
eurjchem-289	304	9	anhydride	anhydride	NOUN
eurjchem-289	304	10	/	/	SYM
eurjchem-289	304	11	sulphuric	sulphuric	ADJ
eurjchem-289	304	12	acid	acid	NOUN
eurjchem-289	304	13	mixture	mixture	NOUN
eurjchem-289	304	14	gave	give	VERB
eurjchem-289	304	15	the	the	DET
eurjchem-289	304	16	required	require	VERB
eurjchem-289	304	17	compounds	compound	NOUN
eurjchem-289	304	18	9a	9a	NOUN
eurjchem-289	304	19	,	,	PUNCT
eurjchem-289	304	20	b	b	X
eurjchem-289	304	21	.	.	PUNCT
eurjchem-289	305	1	ir	ir	PROPN
eurjchem-289	305	2	showed	show	VERB
eurjchem-289	305	3	the	the	DET
eurjchem-289	305	4	absence	absence	NOUN
eurjchem-289	305	5	of	of	ADP
eurjchem-289	305	6	bands	band	NOUN
eurjchem-289	305	7	corresponding	correspond	VERB
eurjchem-289	305	8	to	to	ADP
eurjchem-289	305	9	nh	nh	PROPN
eurjchem-289	305	10	and	and	CCONJ
eurjchem-289	305	11	c	c	NOUN
eurjchem-289	305	12	=	=	NOUN
eurjchem-289	305	13	o	o	NOUN
eurjchem-289	305	14	groups	group	NOUN
eurjchem-289	305	15	.	.	PUNCT
eurjchem-289	306	1	1h	1h	NUM
eurjchem-289	306	2	nmr	nmr	NOUN
eurjchem-289	306	3	spectrum	spectrum	NOUN
eurjchem-289	306	4	revealed	reveal	VERB
eurjchem-289	306	5	the	the	DET
eurjchem-289	306	6	absence	absence	NOUN
eurjchem-289	306	7	of	of	ADP
eurjchem-289	306	8	the	the	DET
eurjchem-289	306	9	singlet	singlet	ADJ
eurjchem-289	306	10	signal	signal	NOUN
eurjchem-289	306	11	of	of	ADP
eurjchem-289	306	12	the	the	DET
eurjchem-289	306	13	vinylic	vinylic	ADJ
eurjchem-289	306	14	proton	proton	NOUN
eurjchem-289	306	15	and	and	CCONJ
eurjchem-289	306	16	the	the	DET
eurjchem-289	306	17	absence	absence	NOUN
eurjchem-289	306	18	of	of	ADP
eurjchem-289	306	19	the	the	DET
eurjchem-289	306	20	exchangeable	exchangeable	ADJ
eurjchem-289	306	21	singlet	singlet	NOUN
eurjchem-289	306	22	signals	signal	NOUN
eurjchem-289	306	23	corresponding	correspond	VERB
eurjchem-289	306	24	to	to	ADP
eurjchem-289	306	25	nh	nh	PROPN
eurjchem-289	306	26	protons	proton	NOUN
eurjchem-289	306	27	.	.	PUNCT
eurjchem-289	307	1	refluxing	refluxing	NOUN
eurjchem-289	307	2	compounds	compound	NOUN
eurjchem-289	307	3	3a	3a	NUM
eurjchem-289	307	4	,	,	PUNCT
eurjchem-289	307	5	c	c	NOUN
eurjchem-289	307	6	with	with	ADP
eurjchem-289	307	7	hydrazine	hydrazine	NOUN
eurjchem-289	307	8	hydrate	hydrate	NOUN
eurjchem-289	307	9	in	in	ADP
eurjchem-289	307	10	ethanol	ethanol	NOUN
eurjchem-289	307	11	containing	contain	VERB
eurjchem-289	307	12	few	few	ADJ
eurjchem-289	307	13	drops	drop	NOUN
eurjchem-289	307	14	of	of	ADP
eurjchem-289	307	15	glacial	glacial	ADJ
eurjchem-289	307	16	acetic	acetic	ADJ
eurjchem-289	307	17	acid	acid	NOUN
eurjchem-289	307	18	afforded	afford	VERB
eurjchem-289	307	19	compounds	compound	NOUN
eurjchem-289	307	20	10a	10a	NOUN
eurjchem-289	307	21	,	,	PUNCT
eurjchem-289	307	22	b	b	X
eurjchem-289	308	1	[	[	X
eurjchem-289	308	2	35	35	NUM
eurjchem-289	308	3	]	]	PUNCT
eurjchem-289	308	4	.	.	PUNCT
eurjchem-289	309	1	mass	mass	PROPN
eurjchem-289	309	2	spectrum	spectrum	NOUN
eurjchem-289	309	3	of	of	ADP
eurjchem-289	309	4	the	the	DET
eurjchem-289	309	5	compound	compound	NOUN
eurjchem-289	309	6	10a	10a	PROPN
eurjchem-289	309	7	showed	show	VERB
eurjchem-289	309	8	molecular	molecular	ADJ
eurjchem-289	309	9	ion	ion	NOUN
eurjchem-289	309	10	peak	peak	NOUN
eurjchem-289	309	11	at	at	ADP
eurjchem-289	309	12	m	m	PROPN
eurjchem-289	309	13	/	/	SYM
eurjchem-289	309	14	z	z	PROPN
eurjchem-289	309	15	302	302	NUM
eurjchem-289	309	16	.	.	PUNCT
eurjchem-289	310	1	1h	1h	NUM
eurjchem-289	310	2	nmr	nmr	NOUN
eurjchem-289	310	3	spectrum	spectrum	NOUN
eurjchem-289	310	4	of	of	ADP
eurjchem-289	310	5	compound	compound	NOUN
eurjchem-289	310	6	10b	10b	NOUN
eurjchem-289	310	7	showed	show	VERB
eurjchem-289	310	8	a	a	DET
eurjchem-289	310	9	singlet	singlet	ADJ
eurjchem-289	310	10	signal	signal	NOUN
eurjchem-289	310	11	at	at	ADP
eurjchem-289	310	12	δ	δ	PROPN
eurjchem-289	310	13	4.27	4.27	NUM
eurjchem-289	310	14	ppm	ppm	NOUN
eurjchem-289	310	15	corresponding	correspond	VERB
eurjchem-289	310	16	to	to	ADP
eurjchem-289	310	17	methylene	methylene	ADJ
eurjchem-289	310	18	protons	proton	NOUN
eurjchem-289	310	19	,	,	PUNCT
eurjchem-289	310	20	a	a	DET
eurjchem-289	310	21	multiplet	multiplet	NOUN
eurjchem-289	310	22	signal	signal	NOUN
eurjchem-289	310	23	at	at	ADP
eurjchem-289	310	24	δ	δ	PROPN
eurjchem-289	310	25	6.77‐8.60	6.77‐8.60	NUM
eurjchem-289	310	26	ppm	ppm	NOUN
eurjchem-289	310	27	corresponding	correspond	VERB
eurjchem-289	310	28	to	to	ADP
eurjchem-289	310	29	the	the	DET
eurjchem-289	310	30	aromatic	aromatic	ADJ
eurjchem-289	310	31	protons	proton	NOUN
eurjchem-289	310	32	and	and	CCONJ
eurjchem-289	310	33	two	two	NUM
eurjchem-289	310	34	exchangeable	exchangeable	ADJ
eurjchem-289	310	35	singlet	singlet	NOUN
eurjchem-289	310	36	signals	signal	NOUN
eurjchem-289	310	37	at	at	ADP
eurjchem-289	310	38	δ	δ	PROPN
eurjchem-289	310	39	12.51	12.51	NUM
eurjchem-289	310	40	and	and	CCONJ
eurjchem-289	310	41	13.06	13.06	NUM
eurjchem-289	310	42	ppm	ppm	NOUN
eurjchem-289	310	43	corresponding	correspond	VERB
eurjchem-289	310	44	to	to	ADP
eurjchem-289	310	45	2	2	NUM
eurjchem-289	310	46	nh	nh	NOUN
eurjchem-289	310	47	protons	proton	NOUN
eurjchem-289	310	48	.	.	PUNCT
eurjchem-289	311	1	reaction	reaction	NOUN
eurjchem-289	311	2	of	of	ADP
eurjchem-289	311	3	compound	compound	NOUN
eurjchem-289	311	4	3a	3a	NUM
eurjchem-289	311	5	,	,	PUNCT
eurjchem-289	311	6	c	c	NOUN
eurjchem-289	311	7	with	with	ADP
eurjchem-289	311	8	hydrazine	hydrazine	NOUN
eurjchem-289	311	9	hydrate	hydrate	NOUN
eurjchem-289	311	10	afforded	afford	VERB
eurjchem-289	311	11	3‐[(5‐aryl‐	3‐[(5‐aryl‐	NUM
eurjchem-289	311	12	1h‐pyrazol‐3‐yl)methyl]‐quinoxalin‐2(1h)‐ones	1h‐pyrazol‐3‐yl)methyl]‐quinoxalin‐2(1h)‐ones	NUM
eurjchem-289	311	13	(	(	PUNCT
eurjchem-289	311	14	10a	10a	NOUN
eurjchem-289	311	15	,	,	PUNCT
eurjchem-289	311	16	b	b	NOUN
eurjchem-289	311	17	)	)	PUNCT
eurjchem-289	311	18	.	.	PUNCT
eurjchem-289	312	1	the	the	DET
eurjchem-289	312	2	proposed	propose	VERB
eurjchem-289	312	3	mechanism	mechanism	NOUN
eurjchem-289	312	4	for	for	ADP
eurjchem-289	312	5	this	this	DET
eurjchem-289	312	6	reaction	reaction	NOUN
eurjchem-289	312	7	may	may	AUX
eurjchem-289	312	8	involve	involve	VERB
eurjchem-289	312	9	either	either	CCONJ
eurjchem-289	312	10	the	the	DET
eurjchem-289	312	11	intermediate	intermediate	ADJ
eurjchem-289	312	12	formation	formation	NOUN
eurjchem-289	312	13	of	of	ADP
eurjchem-289	312	14	hydrazones	hydrazone	NOUN
eurjchem-289	312	15	or	or	CCONJ
eurjchem-289	312	16	the	the	DET
eurjchem-289	312	17	initial	initial	ADJ
eurjchem-289	312	18	micheal	micheal	NOUN
eurjchem-289	312	19	addition	addition	NOUN
eurjchem-289	312	20	of	of	ADP
eurjchem-289	312	21	the	the	DET
eurjchem-289	312	22	hydrazine	hydrazine	NOUN
eurjchem-289	312	23	on	on	ADP
eurjchem-289	312	24	the	the	DET
eurjchem-289	312	25	chalcone	chalcone	NOUN
eurjchem-289	312	26	.	.	PUNCT
eurjchem-289	313	1	coupling	couple	VERB
eurjchem-289	313	2	the	the	DET
eurjchem-289	313	3	alkaline	alkaline	NOUN
eurjchem-289	313	4	solution	solution	NOUN
eurjchem-289	313	5	of	of	ADP
eurjchem-289	313	6	3‐acetonylquinoxalin‐	3‐acetonylquinoxalin‐	NUM
eurjchem-289	313	7	2(1h)‐one	2(1h)‐one	NUM
eurjchem-289	313	8	(	(	PUNCT
eurjchem-289	313	9	2	2	NUM
eurjchem-289	313	10	)	)	PUNCT
eurjchem-289	313	11	with	with	ADP
eurjchem-289	313	12	freshly	freshly	ADV
eurjchem-289	313	13	prepared	prepare	VERB
eurjchem-289	313	14	diazonium	diazonium	NOUN
eurjchem-289	313	15	salts	salt	NOUN
eurjchem-289	313	16	at	at	ADP
eurjchem-289	313	17	ph=	ph=	PROPN
eurjchem-289	313	18	5.0‐5.5	5.0‐5.5	NUM
eurjchem-289	313	19	yielded	yield	VERB
eurjchem-289	313	20	products	product	NOUN
eurjchem-289	313	21	11a	11a	NOUN
eurjchem-289	313	22	,	,	PUNCT
eurjchem-289	313	23	b.	b.	PROPN
eurjchem-289	313	24	ir	ir	PROPN
eurjchem-289	313	25	spectrum	spectrum	PROPN
eurjchem-289	313	26	showed	show	VERB
eurjchem-289	313	27	a	a	DET
eurjchem-289	313	28	band	band	NOUN
eurjchem-289	313	29	at	at	ADP
eurjchem-289	313	30	1380‐1370	1380‐1370	NUM
eurjchem-289	313	31	cm‐1	cm‐1	NOUN
eurjchem-289	313	32	due	due	ADP
eurjchem-289	313	33	to	to	ADP
eurjchem-289	313	34	the	the	DET
eurjchem-289	313	35	bending	bend	VERB
eurjchem-289	313	36	vibration	vibration	NOUN
eurjchem-289	313	37	of	of	ADP
eurjchem-289	313	38	the	the	DET
eurjchem-289	313	39	terminal	terminal	ADJ
eurjchem-289	313	40	methyl	methyl	NOUN
eurjchem-289	313	41	group	group	NOUN
eurjchem-289	313	42	.	.	PUNCT
eurjchem-289	314	1	1h	1h	NUM
eurjchem-289	314	2	nmr	nmr	PROPN
eurjchem-289	314	3	spectra	spectra	NOUN
eurjchem-289	314	4	of	of	ADP
eurjchem-289	314	5	compounds	compound	NOUN
eurjchem-289	314	6	11a	11a	NOUN
eurjchem-289	314	7	showed	show	VERB
eurjchem-289	314	8	a	a	DET
eurjchem-289	314	9	singlet	singlet	ADJ
eurjchem-289	314	10	signal	signal	NOUN
eurjchem-289	314	11	at	at	ADP
eurjchem-289	314	12	δ	δ	PROPN
eurjchem-289	314	13	2.63	2.63	NUM
eurjchem-289	314	14	ppm	ppm	NOUN
eurjchem-289	314	15	corresponding	correspond	VERB
eurjchem-289	314	16	to	to	ADP
eurjchem-289	314	17	the	the	DET
eurjchem-289	314	18	terminal	terminal	ADJ
eurjchem-289	314	19	methyl	methyl	NOUN
eurjchem-289	314	20	group	group	NOUN
eurjchem-289	314	21	and	and	CCONJ
eurjchem-289	314	22	the	the	DET
eurjchem-289	314	23	absence	absence	NOUN
eurjchem-289	314	24	of	of	ADP
eurjchem-289	314	25	the	the	DET
eurjchem-289	314	26	singlet	singlet	ADJ
eurjchem-289	314	27	signal	signal	NOUN
eurjchem-289	314	28	corresponding	correspond	VERB
eurjchem-289	314	29	to	to	ADP
eurjchem-289	314	30	the	the	DET
eurjchem-289	314	31	vinylic	vinylic	ADJ
eurjchem-289	314	32	proton	proton	NOUN
eurjchem-289	314	33	.	.	PUNCT
eurjchem-289	315	1	reaction	reaction	NOUN
eurjchem-289	315	2	of	of	ADP
eurjchem-289	315	3	11a	11a	NOUN
eurjchem-289	315	4	with	with	ADP
eurjchem-289	315	5	bromine	bromine	NOUN
eurjchem-289	315	6	in	in	ADP
eurjchem-289	315	7	acetic	acetic	ADJ
eurjchem-289	315	8	acid	acid	NOUN
eurjchem-289	315	9	containing	contain	VERB
eurjchem-289	315	10	sodium	sodium	NOUN
eurjchem-289	315	11	acetate	acetate	NOUN
eurjchem-289	315	12	yielded	yield	VERB
eurjchem-289	315	13	12	12	NUM
eurjchem-289	315	14	.	.	PUNCT
eurjchem-289	316	1	mass	mass	PROPN
eurjchem-289	316	2	spectrum	spectrum	PROPN
eurjchem-289	316	3	showed	show	VERB
eurjchem-289	316	4	a	a	DET
eurjchem-289	316	5	molecular	molecular	ADJ
eurjchem-289	316	6	ion	ion	NOUN
eurjchem-289	316	7	peak	peak	NOUN
eurjchem-289	316	8	at	at	ADP
eurjchem-289	316	9	m	m	PROPN
eurjchem-289	316	10	/	/	SYM
eurjchem-289	316	11	z	z	PROPN
eurjchem-289	316	12	304	304	NUM
eurjchem-289	316	13	and	and	CCONJ
eurjchem-289	316	14	1h	1h	NUM
eurjchem-289	316	15	nmr	nmr	NOUN
eurjchem-289	316	16	spectrum	spectrum	NOUN
eurjchem-289	316	17	which	which	PRON
eurjchem-289	316	18	revealed	reveal	VERB
eurjchem-289	316	19	a	a	DET
eurjchem-289	316	20	multiplet	multiplet	NOUN
eurjchem-289	316	21	signal	signal	NOUN
eurjchem-289	316	22	at	at	ADP
eurjchem-289	316	23	δ	δ	PROPN
eurjchem-289	316	24	7.33‐8.27	7.33‐8.27	NUM
eurjchem-289	316	25	ppm	ppm	NOUN
eurjchem-289	316	26	corresponding	correspond	VERB
eurjchem-289	316	27	to	to	ADP
eurjchem-289	316	28	the	the	DET
eurjchem-289	316	29	aromatic	aromatic	ADJ
eurjchem-289	316	30	protons	proton	NOUN
eurjchem-289	316	31	,	,	PUNCT
eurjchem-289	316	32	in	in	ADP
eurjchem-289	316	33	addition	addition	NOUN
eurjchem-289	316	34	to	to	ADP
eurjchem-289	316	35	two	two	NUM
eurjchem-289	316	36	exchangeable	exchangeable	ADJ
eurjchem-289	316	37	singlet	singlet	NOUN
eurjchem-289	316	38	signals	signal	NOUN
eurjchem-289	316	39	at	at	ADP
eurjchem-289	316	40	δ	δ	PROPN
eurjchem-289	316	41	11.04	11.04	NUM
eurjchem-289	316	42	and	and	CCONJ
eurjchem-289	316	43	13.27	13.27	NUM
eurjchem-289	316	44	ppm	ppm	NOUN
eurjchem-289	316	45	corresponding	correspond	VERB
eurjchem-289	316	46	to	to	ADP
eurjchem-289	316	47	nh	nh	PROPN
eurjchem-289	316	48	and	and	CCONJ
eurjchem-289	316	49	oh	oh	NUM
eurjchem-289	316	50	protons	proton	NOUN
eurjchem-289	316	51	,	,	PUNCT
eurjchem-289	316	52	respectively	respectively	ADV
eurjchem-289	316	53	[	[	X
eurjchem-289	316	54	36	36	NUM
eurjchem-289	316	55	]	]	PUNCT
eurjchem-289	316	56	.	.	PUNCT
eurjchem-289	317	1	treating	treat	VERB
eurjchem-289	317	2	a	a	DET
eurjchem-289	317	3	solution	solution	NOUN
eurjchem-289	317	4	of	of	ADP
eurjchem-289	317	5	compound	compound	NOUN
eurjchem-289	317	6	2	2	NUM
eurjchem-289	317	7	in	in	ADP
eurjchem-289	317	8	acetic	acetic	ADJ
eurjchem-289	317	9	acid	acid	NOUN
eurjchem-289	317	10	with	with	ADP
eurjchem-289	317	11	solid	solid	ADJ
eurjchem-289	317	12	sodium	sodium	NOUN
eurjchem-289	317	13	nitrite	nitrite	NOUN
eurjchem-289	317	14	,	,	PUNCT
eurjchem-289	317	15	following	follow	VERB
eurjchem-289	317	16	the	the	DET
eurjchem-289	317	17	directions	direction	NOUN
eurjchem-289	317	18	of	of	ADP
eurjchem-289	317	19	shawali	shawali	PROPN
eurjchem-289	317	20	and	and	CCONJ
eurjchem-289	317	21	fahmi	fahmi	PROPN
eurjchem-289	317	22	[	[	X
eurjchem-289	317	23	37	37	NUM
eurjchem-289	317	24	]	]	PUNCT
eurjchem-289	317	25	yielded	yield	VERB
eurjchem-289	317	26	13	13	NUM
eurjchem-289	317	27	whose	whose	DET
eurjchem-289	317	28	structure	structure	NOUN
eurjchem-289	317	29	depends	depend	VERB
eurjchem-289	317	30	on	on	ADP
eurjchem-289	317	31	the	the	DET
eurjchem-289	317	32	position	position	NOUN
eurjchem-289	317	33	at	at	ADP
eurjchem-289	317	34	which	which	PRON
eurjchem-289	317	35	the	the	DET
eurjchem-289	317	36	electrophilic	electrophilic	ADJ
eurjchem-289	317	37	substitution	substitution	NOUN
eurjchem-289	317	38	took	take	VERB
eurjchem-289	317	39	place	place	NOUN
eurjchem-289	317	40	.	.	PUNCT
eurjchem-289	318	1	1h	1h	NUM
eurjchem-289	318	2	nmr	nmr	NOUN
eurjchem-289	318	3	spectrum	spectrum	NOUN
eurjchem-289	318	4	showed	show	VERB
eurjchem-289	318	5	a	a	DET
eurjchem-289	318	6	singlet	singlet	ADJ
eurjchem-289	318	7	signal	signal	NOUN
eurjchem-289	318	8	at	at	ADP
eurjchem-289	318	9	δ	δ	PROPN
eurjchem-289	318	10	2.49	2.49	NUM
eurjchem-289	318	11	ppm	ppm	NOUN
eurjchem-289	318	12	corresponding	correspond	VERB
eurjchem-289	318	13	to	to	ADP
eurjchem-289	318	14	the	the	DET
eurjchem-289	318	15	methyl	methyl	NOUN
eurjchem-289	318	16	protons	proton	NOUN
eurjchem-289	318	17	and	and	CCONJ
eurjchem-289	318	18	the	the	DET
eurjchem-289	318	19	absence	absence	NOUN
eurjchem-289	318	20	of	of	ADP
eurjchem-289	318	21	the	the	DET
eurjchem-289	318	22	singlet	singlet	NOUN
eurjchem-289	318	23	signal	signal	NOUN
eurjchem-289	318	24	at	at	ADP
eurjchem-289	318	25	δ	δ	PROPN
eurjchem-289	318	26	6.01	6.01	NUM
eurjchem-289	318	27	ppm	ppm	NOUN
eurjchem-289	318	28	due	due	ADP
eurjchem-289	318	29	to	to	ADP
eurjchem-289	318	30	the	the	DET
eurjchem-289	318	31	vinylic	vinylic	ADJ
eurjchem-289	318	32	proton	proton	NOUN
eurjchem-289	318	33	.	.	PUNCT
eurjchem-289	319	1	it	it	PRON
eurjchem-289	319	2	was	be	AUX
eurjchem-289	319	3	concluded	conclude	VERB
eurjchem-289	319	4	that	that	SCONJ
eurjchem-289	319	5	the	the	DET
eurjchem-289	319	6	weak	weak	ADJ
eurjchem-289	319	7	non‐bulky	non‐bulky	ADJ
eurjchem-289	319	8	electrophile	electrophile	NOUN
eurjchem-289	319	9	attacked	attack	VERB
eurjchem-289	319	10	the	the	DET
eurjchem-289	319	11	more	more	ADV
eurjchem-289	319	12	activated	activated	ADJ
eurjchem-289	319	13	position	position	NOUN
eurjchem-289	319	14	1	1	NUM
eurjchem-289	319	15	at	at	ADP
eurjchem-289	319	16	the	the	DET
eurjchem-289	319	17	side	side	NOUN
eurjchem-289	319	18	chain	chain	NOUN
eurjchem-289	319	19	.	.	PUNCT
eurjchem-289	320	1	furthermore	furthermore	ADV
eurjchem-289	320	2	,	,	PUNCT
eurjchem-289	320	3	reaction	reaction	NOUN
eurjchem-289	320	4	of	of	ADP
eurjchem-289	320	5	oxime	oxime	NOUN
eurjchem-289	320	6	13	13	NUM
eurjchem-289	320	7	with	with	ADP
eurjchem-289	320	8	benzaldehyde	benzaldehyde	NOUN
eurjchem-289	320	9	in	in	ADP
eurjchem-289	320	10	aqueous	aqueous	ADJ
eurjchem-289	320	11	sodium	sodium	NOUN
eurjchem-289	320	12	hydroxide	hydroxide	NOUN
eurjchem-289	320	13	gave	give	VERB
eurjchem-289	320	14	product	product	NOUN
eurjchem-289	320	15	14	14	NUM
eurjchem-289	320	16	,	,	PUNCT
eurjchem-289	320	17	which	which	PRON
eurjchem-289	320	18	showed	show	VERB
eurjchem-289	320	19	the	the	DET
eurjchem-289	320	20	expected	expect	VERB
eurjchem-289	320	21	molecular	molecular	ADJ
eurjchem-289	320	22	weight	weight	NOUN
eurjchem-289	320	23	at	at	ADP
eurjchem-289	320	24	m	m	PROPN
eurjchem-289	320	25	/	/	SYM
eurjchem-289	320	26	z	z	PROPN
eurjchem-289	320	27	319	319	NUM
eurjchem-289	320	28	.	.	PUNCT
eurjchem-289	321	1	1h	1h	NUM
eurjchem-289	321	2	nmr	nmr	NOUN
eurjchem-289	321	3	spectrum	spectrum	NOUN
eurjchem-289	321	4	showed	show	VERB
eurjchem-289	321	5	a	a	DET
eurjchem-289	321	6	singlet	singlet	ADJ
eurjchem-289	321	7	signal	signal	NOUN
eurjchem-289	321	8	at	at	ADP
eurjchem-289	321	9	δ	δ	PROPN
eurjchem-289	321	10	6.37	6.37	NUM
eurjchem-289	321	11	ppm	ppm	NOUN
eurjchem-289	321	12	.	.	PUNCT
eurjchem-289	322	1	this	this	PRON
eurjchem-289	322	2	suggested	suggest	VERB
eurjchem-289	322	3	an	an	DET
eurjchem-289	322	4	internal	internal	ADJ
eurjchem-289	322	5	micheal	micheal	NOUN
eurjchem-289	322	6	addition	addition	NOUN
eurjchem-289	322	7	of	of	ADP
eurjchem-289	322	8	the	the	DET
eurjchem-289	322	9	oh	oh	PROPN
eurjchem-289	322	10	group	group	NOUN
eurjchem-289	322	11	of	of	ADP
eurjchem-289	322	12	the	the	DET
eurjchem-289	322	13	chalcone	chalcone	NOUN
eurjchem-289	322	14	analogue	analogue	NOUN
eurjchem-289	322	15	on	on	ADP
eurjchem-289	322	16	the	the	DET
eurjchem-289	322	17	c	c	NOUN
eurjchem-289	322	18	=	=	NOUN
eurjchem-289	322	19	c	c	NOUN
eurjchem-289	322	20	to	to	PART
eurjchem-289	322	21	afford	afford	VERB
eurjchem-289	322	22	an	an	DET
eurjchem-289	322	23	oxazine	oxazine	NOUN
eurjchem-289	322	24	ring	ring	NOUN
eurjchem-289	322	25	.	.	PUNCT
eurjchem-289	323	1	one	one	NUM
eurjchem-289	323	2	of	of	ADP
eurjchem-289	323	3	the	the	DET
eurjchem-289	323	4	tested	test	VERB
eurjchem-289	323	5	compounds	compound	NOUN
eurjchem-289	323	6	10a	10a	NOUN
eurjchem-289	323	7	was	be	AUX
eurjchem-289	323	8	found	find	VERB
eurjchem-289	323	9	to	to	PART
eurjchem-289	323	10	exhibit	exhibit	VERB
eurjchem-289	323	11	slight	slight	ADJ
eurjchem-289	323	12	activity	activity	NOUN
eurjchem-289	323	13	against	against	ADP
eurjchem-289	323	14	staphylococcus	staphylococcus	NOUN
eurjchem-289	323	15	aureus	aureus	NOUN
eurjchem-289	323	16	.	.	PUNCT
eurjchem-289	324	1	compounds	compound	VERB
eurjchem-289	324	2	10b	10b	NOUN
eurjchem-289	324	3	,	,	PUNCT
eurjchem-289	324	4	11b	11b	NOUN
eurjchem-289	324	5	and	and	CCONJ
eurjchem-289	324	6	15b	15b	NOUN
eurjchem-289	324	7	showed	show	VERB
eurjchem-289	324	8	slight	slight	ADJ
eurjchem-289	324	9	activity	activity	NOUN
eurjchem-289	324	10	against	against	ADP
eurjchem-289	324	11	escherichia	escherichia	NOUN
eurjchem-289	324	12	coli	coli	NOUN
eurjchem-289	324	13	.	.	PUNCT
eurjchem-289	325	1	unfortunately	unfortunately	ADV
eurjchem-289	325	2	,	,	PUNCT
eurjchem-289	325	3	the	the	DET
eurjchem-289	325	4	rest	rest	NOUN
eurjchem-289	325	5	of	of	ADP
eurjchem-289	325	6	the	the	DET
eurjchem-289	325	7	tested	test	VERB
eurjchem-289	325	8	compounds	compound	NOUN
eurjchem-289	325	9	(	(	PUNCT
eurjchem-289	325	10	3d	3d	NOUN
eurjchem-289	325	11	,	,	PUNCT
eurjchem-289	325	12	4	4	NUM
eurjchem-289	325	13	,	,	PUNCT
eurjchem-289	325	14	5b	5b	NUM
eurjchem-289	325	15	,	,	PUNCT
eurjchem-289	325	16	6c	6c	NUM
eurjchem-289	325	17	,	,	PUNCT
eurjchem-289	325	18	9a,10c,12,13,14a	9a,10c,12,13,14a	NUM
eurjchem-289	325	19	)	)	PUNCT
eurjchem-289	325	20	showed	show	VERB
eurjchem-289	325	21	no	no	DET
eurjchem-289	325	22	inhibition	inhibition	NOUN
eurjchem-289	325	23	against	against	ADP
eurjchem-289	325	24	staphylococcus	staphylococcus	NOUN
eurjchem-289	325	25	aureus	aureus	NOUN
eurjchem-289	325	26	,	,	PUNCT
eurjchem-289	325	27	bacillus	bacillus	NOUN
eurjchem-289	325	28	subtitis	subtitis	NOUN
eurjchem-289	325	29	,	,	PUNCT
eurjchem-289	325	30	escherichia	escherichia	NOUN
eurjchem-289	325	31	coli	coli	NOUN
eurjchem-289	325	32	,	,	PUNCT
eurjchem-289	325	33	pseudo	pseudo	NOUN
eurjchem-289	325	34	aeruginosa	aeruginosa	NOUN
eurjchem-289	325	35	and	and	CCONJ
eurjchem-289	325	36	candida	candida	NOUN
eurjchem-289	325	37	albicans	albican	NOUN
eurjchem-289	325	38	.	.	PUNCT
eurjchem-289	326	1	nineteen	nineteen	NUM
eurjchem-289	326	2	compounds	compound	NOUN
eurjchem-289	326	3	were	be	AUX
eurjchem-289	326	4	screened	screen	VERB
eurjchem-289	326	5	for	for	ADP
eurjchem-289	326	6	their	their	PRON
eurjchem-289	326	7	inhibition	inhibition	NOUN
eurjchem-289	326	8	effect	effect	NOUN
eurjchem-289	326	9	on	on	ADP
eurjchem-289	326	10	ck1	ck1	PROPN
eurjchem-289	326	11	,	,	PUNCT
eurjchem-289	326	12	cdk5	cdk5	PROPN
eurjchem-289	326	13	,	,	PUNCT
eurjchem-289	326	14	and	and	CCONJ
eurjchem-289	326	15	gsk‐3β	gsk‐3β	PROPN
eurjchem-289	326	16	.	.	PUNCT
eurjchem-289	327	1	none	none	NOUN
eurjchem-289	327	2	of	of	ADP
eurjchem-289	327	3	the	the	DET
eurjchem-289	327	4	tested	test	VERB
eurjchem-289	327	5	compounds	compound	NOUN
eurjchem-289	327	6	showed	show	VERB
eurjchem-289	327	7	an	an	DET
eurjchem-289	327	8	inhibition	inhibition	NOUN
eurjchem-289	327	9	activity	activity	NOUN
eurjchem-289	327	10	below	below	ADP
eurjchem-289	327	11	10	10	NUM
eurjchem-289	327	12	µm	µm	ADP
eurjchem-289	327	13	concentration	concentration	NOUN
eurjchem-289	327	14	.	.	PUNCT
eurjchem-289	328	1	acknowledgement	acknowledgement	NOUN
eurjchem-289	328	2	we	we	PRON
eurjchem-289	328	3	are	be	AUX
eurjchem-289	328	4	grateful	grateful	ADJ
eurjchem-289	328	5	to	to	PART
eurjchem-289	328	6	prof	prof	VERB
eurjchem-289	328	7	.	.	PUNCT
eurjchem-289	329	1	dr	dr	PROPN
eurjchem-289	329	2	.	.	PROPN
eurjchem-289	329	3	laurent	laurent	PROPN
eurjchem-289	329	4	meijer	meijer	PROPN
eurjchem-289	329	5	,	,	PUNCT
eurjchem-289	329	6	department	department	NOUN
eurjchem-289	329	7	of	of	ADP
eurjchem-289	329	8	experimental	experimental	ADJ
eurjchem-289	329	9	pathology	pathology	NOUN
eurjchem-289	329	10	,	,	PUNCT
eurjchem-289	329	11	school	school	NOUN
eurjchem-289	329	12	of	of	ADP
eurjchem-289	329	13	medicine	medicine	NOUN
eurjchem-289	329	14	,	,	PUNCT
eurjchem-289	329	15	king	king	NOUN
eurjchem-289	329	16	's	's	PART
eurjchem-289	329	17	college	college	PROPN
eurjchem-289	329	18	london	london	PROPN
eurjchem-289	329	19	,	,	PUNCT
eurjchem-289	329	20	uk	uk	PROPN
eurjchem-289	329	21	.	.	PROPN
eurjchem-289	329	22	for	for	ADP
eurjchem-289	329	23	the	the	DET
eurjchem-289	329	24	biology	biology	NOUN
eurjchem-289	329	25	support	support	NOUN
eurjchem-289	329	26	and	and	CCONJ
eurjchem-289	329	27	providing	provide	VERB
eurjchem-289	329	28	valuable	valuable	ADJ
eurjchem-289	329	29	suggestions	suggestion	NOUN
eurjchem-289	329	30	.	.	PUNCT
eurjchem-289	330	1	also	also	ADV
eurjchem-289	330	2	,	,	PUNCT
eurjchem-289	330	3	we	we	PRON
eurjchem-289	330	4	appreciate	appreciate	VERB
eurjchem-289	330	5	the	the	DET
eurjchem-289	330	6	help	help	NOUN
eurjchem-289	330	7	of	of	ADP
eurjchem-289	330	8	dr	dr	PROPN
eurjchem-289	330	9	.	.	PROPN
eurjchem-289	330	10	ayman	ayman	PROPN
eurjchem-289	330	11	samir	samir	PROPN
eurjchem-289	330	12	yassin	yassin	PROPN
eurjchem-289	330	13	,	,	PUNCT
eurjchem-289	330	14	lecturer	lecturer	NOUN
eurjchem-289	330	15	of	of	ADP
eurjchem-289	330	16	microbiology	microbiology	NOUN
eurjchem-289	330	17	and	and	CCONJ
eurjchem-289	330	18	immunology	immunology	NOUN
eurjchem-289	330	19	,	,	PUNCT
eurjchem-289	330	20	faculty	faculty	NOUN
eurjchem-289	330	21	of	of	ADP
eurjchem-289	330	22	pharmacy	pharmacy	NOUN
eurjchem-289	330	23	,	,	PUNCT
eurjchem-289	330	24	cairo	cairo	PROPN
eurjchem-289	330	25	university	university	PROPN
eurjchem-289	330	26	.	.	PUNCT
eurjchem-289	331	1	references	reference	NOUN
eurjchem-289	331	2	[	[	X
eurjchem-289	331	3	1	1	NUM
eurjchem-289	331	4	]	]	PUNCT
eurjchem-289	331	5	.	.	PUNCT
eurjchem-289	332	1	singh	singh	PROPN
eurjchem-289	332	2	,	,	PUNCT
eurjchem-289	332	3	s.	s.	PROPN
eurjchem-289	332	4	k.	k.	PROPN
eurjchem-289	332	5	;	;	PUNCT
eurjchem-289	332	6	saibaba	saibaba	PROPN
eurjchem-289	332	7	,	,	PUNCT
eurjchem-289	332	8	v.	v.	PROPN
eurjchem-289	332	9	;	;	PUNCT
eurjchem-289	332	10	ravikumar	ravikumar	NOUN
eurjchem-289	332	11	,	,	PUNCT
eurjchem-289	332	12	v.	v.	ADV
eurjchem-289	332	13	;	;	PUNCT
eurjchem-289	332	14	rudrawar	rudrawar	PROPN
eurjchem-289	332	15	,	,	PUNCT
eurjchem-289	332	16	s.	s.	PROPN
eurjchem-289	332	17	v.	v.	PROPN
eurjchem-289	332	18	;	;	PUNCT
eurjchem-289	332	19	daga	daga	NOUN
eurjchem-289	332	20	,	,	PUNCT
eurjchem-289	332	21	p.	p.	NOUN
eurjchem-289	332	22	;	;	PUNCT
eurjchem-289	332	23	rao	rao	PROPN
eurjchem-289	332	24	,	,	PUNCT
eurjchem-289	332	25	c.	c.	PROPN
eurjchem-289	332	26	s.	s.	PROPN
eurjchem-289	332	27	;	;	PUNCT
eurjchem-289	332	28	akhila	akhila	NOUN
eurjchem-289	332	29	,	,	PUNCT
eurjchem-289	332	30	v.	v.	PROPN
eurjchem-289	332	31	;	;	PUNCT
eurjchem-289	332	32	hegde	hegde	PROPN
eurjchem-289	332	33	,	,	PUNCT
eurjchem-289	332	34	p.	p.	PROPN
eurjchem-289	332	35	;	;	PUNCT
eurjchem-289	332	36	rao	rao	PROPN
eurjchem-289	332	37	,	,	PUNCT
eurjchem-289	332	38	y.	y.	PROPN
eurjchem-289	332	39	k.	k.	PROPN
eurjchem-289	332	40	bioorg	bioorg	PROPN
eurjchem-289	332	41	.	.	PUNCT
eurjchem-289	333	1	med	med	PROPN
eurjchem-289	333	2	.	.	PROPN
eurjchem-289	333	3	chem	chem	PROPN
eurjchem-289	333	4	.	.	PUNCT
eurjchem-289	334	1	2004	2004	NUM
eurjchem-289	334	2	,	,	PUNCT
eurjchem-289	334	3	12	12	NUM
eurjchem-289	334	4	,	,	PUNCT
eurjchem-289	334	5	1881‐1893	1881‐1893	NUM
eurjchem-289	334	6	.	.	PUNCT
eurjchem-289	335	1	shabaan	shabaan	PROPN
eurjchem-289	335	2	et	et	PROPN
eurjchem-289	335	3	al	al	PROPN
eurjchem-289	335	4	.	.	PUNCT
eurjchem-289	335	5	/	/	SYM
eurjchem-289	335	6	european	european	PROPN
eurjchem-289	335	7	journal	journal	PROPN
eurjchem-289	335	8	of	of	ADP
eurjchem-289	335	9	chemistry	chemistry	NOUN
eurjchem-289	335	10	2	2	NUM
eurjchem-289	335	11	(	(	PUNCT
eurjchem-289	335	12	3	3	NUM
eurjchem-289	335	13	)	)	PUNCT
eurjchem-289	335	14	(	(	PUNCT
eurjchem-289	335	15	2011	2011	NUM
eurjchem-289	335	16	)	)	PUNCT
eurjchem-289	335	17	365‐371	365‐371	NUM
eurjchem-289	335	18	371	371	NUM
eurjchem-289	336	1	[	[	X
eurjchem-289	336	2	2	2	NUM
eurjchem-289	336	3	]	]	PUNCT
eurjchem-289	336	4	.	.	PUNCT
eurjchem-289	337	1	burguete	burguete	PROPN
eurjchem-289	337	2	,	,	PUNCT
eurjchem-289	337	3	a.	a.	NOUN
eurjchem-289	337	4	;	;	PUNCT
eurjchem-289	337	5	pontiki	pontiki	PROPN
eurjchem-289	337	6	,	,	PUNCT
eurjchem-289	337	7	e.	e.	PROPN
eurjchem-289	337	8	;	;	PUNCT
eurjchem-289	337	9	hadjipavlou‐litina	hadjipavlou‐litina	PROPN
eurjchem-289	337	10	,	,	PUNCT
eurjchem-289	337	11	d.	d.	PROPN
eurjchem-289	337	12	;	;	PUNCT
eurjchem-289	337	13	villar	villar	PROPN
eurjchem-289	337	14	,	,	PUNCT
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eurjchem-289	337	16	;	;	PUNCT
eurjchem-289	337	17	vicente	vicente	PROPN
eurjchem-289	337	18	,	,	PUNCT
eurjchem-289	337	19	e.	e.	PROPN
eurjchem-289	337	20	;	;	PUNCT
eurjchem-289	337	21	solano	solano	PROPN
eurjchem-289	337	22	,	,	PUNCT
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eurjchem-289	337	25	ancizu	ancizu	PROPN
eurjchem-289	337	26	,	,	PUNCT
eurjchem-289	337	27	s.	s.	PROPN
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eurjchem-289	337	29	perez‐silanes	perez‐silanes	PROPN
eurjchem-289	337	30	,	,	PUNCT
eurjchem-289	337	31	s.	s.	PROPN
eurjchem-289	337	32	;	;	PUNCT
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eurjchem-289	337	34	,	,	PUNCT
eurjchem-289	337	35	i.	i.	PROPN
eurjchem-289	337	36	;	;	PUNCT
eurjchem-289	337	37	monge	monge	PROPN
eurjchem-289	337	38	,	,	PUNCT
eurjchem-289	337	39	a.	a.	NOUN
eurjchem-289	337	40	bioorg	bioorg	PROPN
eurjchem-289	337	41	.	.	PUNCT
eurjchem-289	338	1	med	med	PROPN
eurjchem-289	338	2	.	.	PROPN
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eurjchem-289	339	2	.	.	PUNCT
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eurjchem-289	340	2	,	,	PUNCT
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eurjchem-289	340	4	,	,	PUNCT
eurjchem-289	340	5	6439‐6443	6439‐6443	NUM
eurjchem-289	340	6	.	.	PUNCT
eurjchem-289	341	1	[	[	X
eurjchem-289	341	2	3	3	NUM
eurjchem-289	341	3	]	]	PUNCT
eurjchem-289	341	4	.	.	PUNCT
eurjchem-289	342	1	carta	carta	PROPN
eurjchem-289	342	2	,	,	PUNCT
eurjchem-289	342	3	a.	a.	NOUN
eurjchem-289	342	4	;	;	PUNCT
eurjchem-289	342	5	loriga	loriga	NOUN
eurjchem-289	342	6	,	,	PUNCT
eurjchem-289	342	7	m.	m.	NOUN
eurjchem-289	342	8	;	;	PUNCT
eurjchem-289	342	9	paglitti	paglitti	PROPN
eurjchem-289	342	10	,	,	PUNCT
eurjchem-289	342	11	g.	g.	PROPN
eurjchem-289	342	12	;	;	PUNCT
eurjchem-289	342	13	mattana	mattana	PROPN
eurjchem-289	342	14	,	,	PUNCT
eurjchem-289	342	15	a.	a.	NOUN
eurjchem-289	342	16	;	;	PUNCT
eurjchem-289	342	17	fiori	fiori	NOUN
eurjchem-289	342	18	,	,	PUNCT
eurjchem-289	342	19	p.	p.	NOUN
eurjchem-289	342	20	;	;	PUNCT
eurjchem-289	342	21	mollicotti	mollicotti	VERB
eurjchem-289	342	22	,	,	PUNCT
eurjchem-289	342	23	p.	p.	NOUN
eurjchem-289	342	24	;	;	PUNCT
eurjchem-289	342	25	sechi	sechi	PROPN
eurjchem-289	342	26	,	,	PUNCT
eurjchem-289	342	27	l.	l.	PROPN
eurjchem-289	342	28	;	;	PUNCT
eurjchem-289	342	29	zanetti	zanetti	PROPN
eurjchem-289	342	30	,	,	PUNCT
eurjchem-289	342	31	s.	s.	PROPN
eurjchem-289	342	32	eur	eur	PROPN
eurjchem-289	342	33	.	.	PUNCT
eurjchem-289	343	1	j.	j.	PROPN
eurjchem-289	343	2	med	med	PROPN
eurjchem-289	343	3	.	.	PROPN
eurjchem-289	343	4	chem	chem	PROPN
eurjchem-289	343	5	.	.	PUNCT
eurjchem-289	344	1	2004	2004	NUM
eurjchem-289	344	2	,	,	PUNCT
eurjchem-289	344	3	39	39	NUM
eurjchem-289	344	4	,	,	PUNCT
eurjchem-289	344	5	195‐203	195‐203	NUM
eurjchem-289	344	6	.	.	PUNCT
eurjchem-289	345	1	[	[	X
eurjchem-289	345	2	4	4	NUM
eurjchem-289	345	3	]	]	PUNCT
eurjchem-289	345	4	.	.	PUNCT
eurjchem-289	346	1	jaso	jaso	PROPN
eurjchem-289	346	2	,	,	PUNCT
eurjchem-289	346	3	a.	a.	PROPN
eurjchem-289	346	4	;	;	PUNCT
eurjchem-289	346	5	zarranz	zarranz	PROPN
eurjchem-289	346	6	,	,	PUNCT
eurjchem-289	346	7	b.	b.	PROPN
eurjchem-289	346	8	;	;	PUNCT
eurjchem-289	346	9	aldana	aldana	PROPN
eurjchem-289	346	10	,	,	PUNCT
eurjchem-289	346	11	i.	i.	PROPN
eurjchem-289	346	12	;	;	PUNCT
eurjchem-289	346	13	monge	monge	PROPN
eurjchem-289	346	14	,	,	PUNCT
eurjchem-289	346	15	a.	a.	PROPN
eurjchem-289	346	16	j.	j.	PROPN
eurjchem-289	346	17	med	med	PROPN
eurjchem-289	346	18	.	.	PROPN
eurjchem-289	346	19	chem	chem	PROPN
eurjchem-289	346	20	.	.	PUNCT
eurjchem-289	347	1	2005	2005	NUM
eurjchem-289	347	2	,	,	PUNCT
eurjchem-289	347	3	48	48	NUM
eurjchem-289	347	4	,	,	PUNCT
eurjchem-289	347	5	2019‐	2019‐	NUM
eurjchem-289	347	6	2025	2025	NUM
eurjchem-289	347	7	.	.	PUNCT
eurjchem-289	348	1	[	[	X
eurjchem-289	348	2	5	5	NUM
eurjchem-289	348	3	]	]	PUNCT
eurjchem-289	348	4	.	.	PUNCT
eurjchem-289	348	5	badran	badran	PROPN
eurjchem-289	348	6	,	,	PUNCT
eurjchem-289	348	7	m.	m.	NOUN
eurjchem-289	348	8	;	;	PUNCT
eurjchem-289	348	9	moneer	moneer	NOUN
eurjchem-289	348	10	,	,	PUNCT
eurjchem-289	348	11	a.	a.	NOUN
eurjchem-289	348	12	;	;	PUNCT
eurjchem-289	348	13	refaat	refaat	PROPN
eurjchem-289	348	14	,	,	PUNCT
eurjchem-289	348	15	h.	h.	PROPN
eurjchem-289	348	16	m.	m.	PROPN
eurjchem-289	348	17	;	;	PUNCT
eurjchem-289	348	18	el‐malah	el‐malah	PROPN
eurjchem-289	348	19	,	,	PUNCT
eurjchem-289	348	20	a.	a.	PROPN
eurjchem-289	348	21	j.	j.	PROPN
eurjchem-289	348	22	chinese	chinese	PROPN
eurjchem-289	348	23	chem	chem	PROPN
eurjchem-289	348	24	.	.	PUNCT
eurjchem-289	349	1	soc	soc	PROPN
eurjchem-289	349	2	.	.	PUNCT
eurjchem-289	350	1	2007	2007	NUM
eurjchem-289	350	2	,	,	PUNCT
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eurjchem-289	350	4	,	,	PUNCT
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eurjchem-289	350	6	.	.	PUNCT
eurjchem-289	351	1	[	[	X
eurjchem-289	351	2	6	6	NUM
eurjchem-289	351	3	]	]	PUNCT
eurjchem-289	351	4	.	.	PUNCT
eurjchem-289	351	5	badran	badran	PROPN
eurjchem-289	351	6	,	,	PUNCT
eurjchem-289	351	7	m.	m.	NOUN
eurjchem-289	351	8	;	;	PUNCT
eurjchem-289	351	9	abouzid	abouzid	PROPN
eurjchem-289	351	10	,	,	PUNCT
eurjchem-289	351	11	k.	k.	PROPN
eurjchem-289	351	12	;	;	PUNCT
eurjchem-289	351	13	hussein	hussein	PROPN
eurjchem-289	351	14	,	,	PUNCT
eurjchem-289	351	15	m.	m.	PROPN
eurjchem-289	351	16	h.	h.	PROPN
eurjchem-289	351	17	arch	arch	PROPN
eurjchem-289	351	18	.	.	PUNCT
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eurjchem-289	352	2	.	.	PUNCT
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eurjchem-289	353	2	.	.	PROPN
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eurjchem-289	353	4	,	,	PUNCT
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eurjchem-289	353	6	,	,	PUNCT
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eurjchem-289	353	8	.	.	PUNCT
eurjchem-289	354	1	[	[	X
eurjchem-289	354	2	7	7	NUM
eurjchem-289	354	3	]	]	PUNCT
eurjchem-289	354	4	.	.	PUNCT
eurjchem-289	355	1	grande	grande	PROPN
eurjchem-289	355	2	,	,	PUNCT
eurjchem-289	355	3	f.	f.	PROPN
eurjchem-289	355	4	;	;	PUNCT
eurjchem-289	355	5	aiello	aiello	PROPN
eurjchem-289	355	6	,	,	PUNCT
eurjchem-289	355	7	f.	f.	PROPN
eurjchem-289	355	8	;	;	PUNCT
eurjchem-289	355	9	de	de	PROPN
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eurjchem-289	355	11	,	,	PUNCT
eurjchem-289	355	12	o.	o.	PROPN
eurjchem-289	355	13	;	;	PUNCT
eurjchem-289	355	14	brizzi	brizzi	NOUN
eurjchem-289	355	15	,	,	PUNCT
eurjchem-289	355	16	a.	a.	NOUN
eurjchem-289	355	17	;	;	PUNCT
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eurjchem-289	355	19	,	,	PUNCT
eurjchem-289	355	20	a.	a.	NOUN
eurjchem-289	355	21	;	;	PUNCT
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eurjchem-289	355	23	,	,	PUNCT
eurjchem-289	355	24	n.	n.	PROPN
eurjchem-289	355	25	bioorg	bioorg	PROPN
eurjchem-289	355	26	.	.	PUNCT
eurjchem-289	356	1	med	med	PROPN
eurjchem-289	356	2	.	.	PROPN
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eurjchem-289	356	4	.	.	PUNCT
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eurjchem-289	357	2	,	,	PUNCT
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eurjchem-289	357	4	,	,	PUNCT
eurjchem-289	357	5	288‐294	288‐294	NUM
eurjchem-289	357	6	.	.	PUNCT
eurjchem-289	358	1	[	[	X
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eurjchem-289	358	3	]	]	PUNCT
eurjchem-289	358	4	.	.	PUNCT
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eurjchem-289	359	2	,	,	PUNCT
eurjchem-289	359	3	g.	g.	PROPN
eurjchem-289	359	4	;	;	PUNCT
eurjchem-289	359	5	deleuze‐masquefa	deleuze‐masquefa	PROPN
eurjchem-289	359	6	,	,	PUNCT
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eurjchem-289	359	8	;	;	PUNCT
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eurjchem-289	359	12	;	;	PUNCT
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eurjchem-289	359	14	,	,	PUNCT
eurjchem-289	359	15	s.	s.	PROPN
eurjchem-289	359	16	;	;	PUNCT
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eurjchem-289	359	19	j.	j.	PROPN
eurjchem-289	359	20	;	;	PUNCT
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eurjchem-289	359	22	,	,	PUNCT
eurjchem-289	359	23	f.	f.	PROPN
eurjchem-289	359	24	;	;	PUNCT
eurjchem-289	359	25	pinguet	pinguet	PROPN
eurjchem-289	359	26	.	.	PUNCT
eurjchem-289	360	1	f.	f.	PROPN
eurjchem-289	360	2	;	;	PUNCT
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eurjchem-289	360	4	,	,	PUNCT
eurjchem-289	360	5	p.	p.	NOUN
eurjchem-289	360	6	bioorg	bioorg	PROPN
eurjchem-289	360	7	.	.	PUNCT
eurjchem-289	361	1	med	med	PROPN
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eurjchem-289	361	4	.	.	PUNCT
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eurjchem-289	362	2	,	,	PUNCT
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eurjchem-289	362	4	,	,	PUNCT
eurjchem-289	362	5	6601‐6610	6601‐6610	NUM
eurjchem-289	362	6	.	.	PUNCT
eurjchem-289	363	1	[	[	X
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eurjchem-289	363	3	]	]	PUNCT
eurjchem-289	363	4	.	.	PUNCT
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eurjchem-289	363	6	,	,	PUNCT
eurjchem-289	363	7	e.	e.	PROPN
eurjchem-289	363	8	;	;	PUNCT
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eurjchem-289	363	10	,	,	PUNCT
eurjchem-289	363	11	l.	l.	PROPN
eurjchem-289	363	12	;	;	PUNCT
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eurjchem-289	363	14	,	,	PUNCT
eurjchem-289	363	15	e.	e.	PROPN
eurjchem-289	363	16	;	;	PUNCT
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eurjchem-289	363	34	,	,	PUNCT
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eurjchem-289	363	36	;	;	PUNCT
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eurjchem-289	363	38	,	,	PUNCT
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eurjchem-289	363	42	,	,	PUNCT
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eurjchem-289	363	46	,	,	PUNCT
eurjchem-289	363	47	a.	a.	PROPN
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eurjchem-289	364	1	j.	j.	PROPN
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eurjchem-289	364	5	.	.	PUNCT
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eurjchem-289	365	2	,	,	PUNCT
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eurjchem-289	365	4	,	,	PUNCT
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eurjchem-289	365	6	.	.	PUNCT
eurjchem-289	366	1	[	[	X
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eurjchem-289	366	3	]	]	PUNCT
eurjchem-289	366	4	.	.	PUNCT
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eurjchem-289	367	2	,	,	PUNCT
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eurjchem-289	367	4	;	;	PUNCT
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eurjchem-289	367	6	,	,	PUNCT
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eurjchem-289	367	8	;	;	PUNCT
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eurjchem-289	367	13	;	;	PUNCT
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eurjchem-289	367	17	;	;	PUNCT
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eurjchem-289	367	23	.	.	PUNCT
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eurjchem-289	369	1	lett	lett	PROPN
eurjchem-289	369	2	.	.	PUNCT
eurjchem-289	370	1	2010	2010	NUM
eurjchem-289	370	2	,	,	PUNCT
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eurjchem-289	370	4	,	,	PUNCT
eurjchem-289	370	5	6773‐6776	6773‐6776	NUM
eurjchem-289	370	6	.	.	PUNCT
eurjchem-289	371	1	[	[	X
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eurjchem-289	371	3	]	]	PUNCT
eurjchem-289	371	4	.	.	PUNCT
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eurjchem-289	372	2	,	,	PUNCT
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eurjchem-289	372	4	;	;	PUNCT
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eurjchem-289	372	10	,	,	PUNCT
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eurjchem-289	372	20	;	;	PUNCT
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eurjchem-289	374	3	]	]	PUNCT
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eurjchem-289	377	2	,	,	PUNCT
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eurjchem-289	378	3	]	]	PUNCT
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eurjchem-289	380	2	,	,	PUNCT
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eurjchem-289	380	4	)	)	PUNCT
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eurjchem-289	381	3	]	]	PUNCT
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eurjchem-289	382	3	]	]	PUNCT
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eurjchem-289	384	2	.	.	PUNCT
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eurjchem-289	385	2	,	,	PUNCT
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eurjchem-289	386	3	]	]	PUNCT
eurjchem-289	386	4	.	.	PUNCT
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eurjchem-289	387	2	,	,	PUNCT
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eurjchem-289	387	7	,	,	PUNCT
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eurjchem-289	387	17	.	.	PUNCT
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eurjchem-289	388	2	.	.	PUNCT
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eurjchem-289	389	2	,	,	PUNCT
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eurjchem-289	389	4	,	,	PUNCT
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eurjchem-289	389	7	.	.	PUNCT
eurjchem-289	390	1	[	[	X
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eurjchem-289	390	3	]	]	PUNCT
eurjchem-289	390	4	.	.	PUNCT
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eurjchem-289	391	2	,	,	PUNCT
eurjchem-289	391	3	l.	l.	PROPN
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eurjchem-289	391	5	;	;	PUNCT
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eurjchem-289	391	8	m.	m.	PROPN
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eurjchem-289	391	10	;	;	PUNCT
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eurjchem-289	393	8	.	.	PUNCT
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eurjchem-289	394	4	.	.	PUNCT
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eurjchem-289	395	2	,	,	PUNCT
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eurjchem-289	395	5	;	;	PUNCT
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eurjchem-289	395	7	,	,	PUNCT
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eurjchem-289	395	46	.	.	PUNCT
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eurjchem-289	397	2	.	.	PUNCT
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eurjchem-289	398	2	.	.	PROPN
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eurjchem-289	398	8	.	.	PUNCT
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eurjchem-289	399	4	.	.	PUNCT
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eurjchem-289	400	2	,	,	PUNCT
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eurjchem-289	401	2	,	,	PUNCT
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eurjchem-289	402	4	.	.	PUNCT
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eurjchem-289	403	6	,	,	PUNCT
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eurjchem-289	403	8	;	;	PUNCT
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eurjchem-289	404	2	.	.	PUNCT
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eurjchem-289	405	7	.	.	PUNCT
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eurjchem-289	410	4	.	.	PUNCT
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eurjchem-289	411	36	h.	h.	PROPN
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eurjchem-289	411	39	xiaoling	xiaoling	PROPN
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eurjchem-289	411	42	;	;	PUNCT
eurjchem-289	411	43	norman	norman	PROPN
eurjchem-289	411	44	,	,	PUNCT
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eurjchem-289	413	2	.	.	PUNCT
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eurjchem-289	414	2	,	,	PUNCT
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eurjchem-289	414	4	,	,	PUNCT
eurjchem-289	414	5	5384‐5389	5384‐5389	NUM
eurjchem-289	414	6	.	.	PUNCT
eurjchem-289	415	1	[	[	X
eurjchem-289	415	2	23	23	NUM
eurjchem-289	415	3	]	]	PUNCT
eurjchem-289	415	4	.	.	PUNCT
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eurjchem-289	416	2	,	,	PUNCT
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eurjchem-289	417	2	.	.	PUNCT
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eurjchem-289	418	2	.	.	PUNCT
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eurjchem-289	419	2	,	,	PUNCT
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eurjchem-289	419	4	,	,	PUNCT
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eurjchem-289	419	6	.	.	PUNCT
eurjchem-289	420	1	[	[	X
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eurjchem-289	420	3	]	]	PUNCT
eurjchem-289	420	4	.	.	PUNCT
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eurjchem-289	421	5	.	.	PUNCT
eurjchem-289	422	1	chim	chim	PROPN
eurjchem-289	422	2	.	.	PUNCT
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eurjchem-289	423	2	.	.	PUNCT
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eurjchem-289	424	2	,	,	PUNCT
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eurjchem-289	424	4	,	,	PUNCT
eurjchem-289	424	5	612‐619	612‐619	NUM
eurjchem-289	424	6	.	.	PUNCT
eurjchem-289	425	1	[	[	X
eurjchem-289	425	2	25	25	NUM
eurjchem-289	425	3	]	]	PUNCT
eurjchem-289	425	4	.	.	PUNCT
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eurjchem-289	427	2	.	.	PUNCT
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eurjchem-289	428	2	.	.	PROPN
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eurjchem-289	428	4	,	,	PUNCT
eurjchem-289	428	5	10	10	NUM
eurjchem-289	428	6	,	,	PUNCT
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eurjchem-289	428	8	.	.	PUNCT
eurjchem-289	429	1	[	[	X
eurjchem-289	429	2	26	26	NUM
eurjchem-289	429	3	]	]	PUNCT
eurjchem-289	429	4	.	.	PUNCT
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eurjchem-289	430	4	;	;	PUNCT
eurjchem-289	430	5	el‐masry	el‐masry	PROPN
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eurjchem-289	430	8	;	;	PUNCT
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eurjchem-289	430	12	;	;	PUNCT
eurjchem-289	430	13	amer	amer	PROPN
eurjchem-289	430	14	,	,	PUNCT
eurjchem-289	430	15	a.	a.	PROPN
eurjchem-289	430	16	;	;	PUNCT
eurjchem-289	430	17	zimmer	zimmer	PROPN
eurjchem-289	430	18	,	,	PUNCT
eurjchem-289	430	19	h.	h.	PROPN
eurjchem-289	430	20	j.	j.	PROPN
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eurjchem-289	430	23	.	.	PUNCT
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eurjchem-289	431	2	,	,	PUNCT
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eurjchem-289	431	4	,	,	PUNCT
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eurjchem-289	431	6	.	.	PUNCT
eurjchem-289	432	1	[	[	X
eurjchem-289	432	2	27	27	NUM
eurjchem-289	432	3	]	]	SYM
eurjchem-289	432	4	.	.	PUNCT
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eurjchem-289	432	6	,	,	PUNCT
eurjchem-289	432	7	l.	l.	PROPN
eurjchem-289	432	8	;	;	PUNCT
eurjchem-289	432	9	thunnissen	thunnissen	PROPN
eurjchem-289	432	10	,	,	PUNCT
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eurjchem-289	432	12	;	;	PUNCT
eurjchem-289	432	13	white	white	ADJ
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eurjchem-289	432	19	,	,	PUNCT
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eurjchem-289	432	28	l.	l.	PROPN
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eurjchem-289	432	37	k.	k.	PROPN
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eurjchem-289	432	40	salinas	salinas	PROPN
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eurjchem-289	432	46	,	,	PUNCT
eurjchem-289	432	47	y.	y.	PROPN
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eurjchem-289	432	50	biernat	biernat	ADJ
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eurjchem-289	433	1	[	[	X
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eurjchem-289	433	3	]	]	SYM
eurjchem-289	433	4	.	.	PUNCT
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eurjchem-289	434	2	,	,	PUNCT
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eurjchem-289	434	4	;	;	PUNCT
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eurjchem-289	434	6	,	,	PUNCT
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eurjchem-289	435	1	j.	j.	PROPN
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eurjchem-289	435	3	.	.	PUNCT
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eurjchem-289	436	2	,	,	PUNCT
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eurjchem-289	436	4	,	,	PUNCT
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eurjchem-289	436	6	.	.	PUNCT
eurjchem-289	437	1	[	[	X
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eurjchem-289	437	3	]	]	PUNCT
eurjchem-289	437	4	.	.	PUNCT
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eurjchem-289	438	4	;	;	PUNCT
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eurjchem-289	439	2	.	.	PUNCT
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eurjchem-289	440	2	,	,	PUNCT
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eurjchem-289	440	4	,	,	PUNCT
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eurjchem-289	440	6	.	.	PUNCT
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eurjchem-289	441	4	.	.	PUNCT
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eurjchem-289	442	8	;	;	PUNCT
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eurjchem-289	443	2	.	.	PUNCT
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eurjchem-289	444	2	.	.	PUNCT
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eurjchem-289	445	2	.	.	PUNCT
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eurjchem-289	446	2	,	,	PUNCT
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eurjchem-289	446	6	.	.	PUNCT
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eurjchem-289	450	2	.	.	PUNCT
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eurjchem-289	455	4	;	;	PUNCT
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eurjchem-289	455	8	;	;	PUNCT
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eurjchem-289	456	2	,	,	PUNCT
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eurjchem-289	456	6	.	.	PUNCT
eurjchem-289	457	1	[	[	X
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eurjchem-289	457	3	]	]	PUNCT
eurjchem-289	457	4	.	.	PUNCT
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eurjchem-289	459	4	.	.	PUNCT
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eurjchem-289	460	4	;	;	PUNCT
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eurjchem-289	460	8	;	;	PUNCT
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eurjchem-289	460	22	.	.	PUNCT
eurjchem-289	461	1	pharm	pharm	NOUN
eurjchem-289	461	2	.	.	PUNCT
eurjchem-289	462	1	2003	2003	NUM
eurjchem-289	462	2	,	,	PUNCT
eurjchem-289	462	3	336	336	NUM
eurjchem-289	462	4	,	,	PUNCT
eurjchem-289	462	5	362‐371	362‐371	NUM
eurjchem-289	462	6	.	.	PUNCT
eurjchem-289	463	1	[	[	X
eurjchem-289	463	2	36	36	NUM
eurjchem-289	463	3	]	]	PUNCT
eurjchem-289	463	4	.	.	PUNCT
eurjchem-289	464	1	kandeel	kandeel	PROPN
eurjchem-289	464	2	,	,	PUNCT
eurjchem-289	464	3	m.	m.	NOUN
eurjchem-289	464	4	;	;	PUNCT
eurjchem-289	464	5	omar	omar	PROPN
eurjchem-289	464	6	,	,	PUNCT
eurjchem-289	464	7	a.	a.	NOUN
eurjchem-289	464	8	h.	h.	PROPN
eurjchem-289	464	9	bull	bull	PROPN
eurjchem-289	464	10	.	.	PUNCT
eurjchem-289	465	1	fac	fac	PROPN
eurjchem-289	465	2	.	.	PUNCT
eurjchem-289	466	1	pharm	pharm	PROPN
eurjchem-289	466	2	.	.	PUNCT
eurjchem-289	467	1	cairo	cairo	PROPN
eurjchem-289	467	2	univ	univ	PROPN
eurjchem-289	467	3	.	.	PROPN
eurjchem-289	468	1	2003	2003	NUM
eurjchem-289	468	2	,	,	PUNCT
eurjchem-289	468	3	41	41	NUM
eurjchem-289	468	4	,	,	PUNCT
eurjchem-289	468	5	43‐50	43‐50	NUM
eurjchem-289	468	6	.	.	PUNCT
eurjchem-289	469	1	[	[	X
eurjchem-289	469	2	37	37	NUM
eurjchem-289	469	3	]	]	PUNCT
eurjchem-289	469	4	.	.	PUNCT
eurjchem-289	469	5	shawali	shawali	PROPN
eurjchem-289	469	6	,	,	PUNCT
eurjchem-289	469	7	a.	a.	NOUN
eurjchem-289	469	8	;	;	PUNCT
eurjchem-289	469	9	fahmi	fahmi	PROPN
eurjchem-289	469	10	,	,	PUNCT
eurjchem-289	469	11	a.	a.	PROPN
eurjchem-289	469	12	ind	ind	PROPN
eurjchem-289	469	13	.	.	PUNCT
eurjchem-289	470	1	j.	j.	PROPN
eurjchem-289	470	2	chem	chem	PROPN
eurjchem-289	470	3	.	.	PUNCT
eurjchem-289	471	1	1975	1975	NUM
eurjchem-289	471	2	,	,	PUNCT
eurjchem-289	471	3	13	13	NUM
eurjchem-289	471	4	,	,	PUNCT
eurjchem-289	471	5	105‐109	105‐109	NUM
eurjchem-289	471	6	.	.	PUNCT