id sid tid token lemma pos eurjchem-29 1 1 microsoft microsoft PROPN eurjchem-29 1 2 word word NOUN eurjchem-29 1 3 european_journal_of_chemistry_1_3_2010_168_172_29 european_journal_of_chemistry_1_3_2010_168_172_29 PROPN eurjchem-29 1 4 european european ADJ eurjchem-29 1 5     SPACE eurjchem-29 1 6 journal journal NOUN eurjchem-29 1 7     SPACE eurjchem-29 1 8 of of ADP eurjchem-29 1 9     SPACE eurjchem-29 1 10 chemistry chemistry NOUN eurjchem-29 1 11     SPACE eurjchem-29 1 12 1 1 NUM eurjchem-29 1 13     SPACE eurjchem-29 1 14 ( ( PUNCT eurjchem-29 1 15 3 3 NUM eurjchem-29 1 16 ) ) PUNCT eurjchem-29 1 17     SPACE eurjchem-29 1 18 ( ( PUNCT eurjchem-29 1 19 2010 2010 NUM eurjchem-29 1 20 ) ) PUNCT eurjchem-29 1 21     SPACE eurjchem-29 1 22 168‐172 168‐172 NUM eurjchem-29 1 23         SPACE eurjchem-29 1 24 european european ADJ eurjchem-29 1 25     SPACE eurjchem-29 1 26 journal journal NOUN eurjchem-29 1 27     SPACE eurjchem-29 1 28 of of ADP eurjchem-29 1 29     SPACE eurjchem-29 1 30 chemistry chemistry NOUN eurjchem-29 1 31     SPACE eurjchem-29 1 32 issn issn VERB eurjchem-29 1 33     SPACE eurjchem-29 1 34 2153‐2249 2153‐2249 NUM eurjchem-29 1 35     SPACE eurjchem-29 1 36 ( ( PUNCT eurjchem-29 1 37 print print NOUN eurjchem-29 1 38 ) ) PUNCT eurjchem-29 1 39     SPACE eurjchem-29 1 40 / / SYM eurjchem-29 1 41     SPACE eurjchem-29 1 42 issn issn VERB eurjchem-29 1 43     SPACE eurjchem-29 1 44 2153‐2257 2153‐2257 NUM eurjchem-29 1 45     SPACE eurjchem-29 1 46 ( ( PUNCT eurjchem-29 1 47 online online ADJ eurjchem-29 1 48 ) ) PUNCT eurjchem-29 1 49     SPACE eurjchem-29 1 50   NOUN eurjchem-29 1 51     SPACE eurjchem-29 1 52 2010 2010 NUM eurjchem-29 1 53     SPACE eurjchem-29 1 54 eurjchem eurjchem NOUN eurjchem-29 1 55     SPACE eurjchem-29 1 56 doi:10.5155 doi:10.5155 PROPN eurjchem-29 1 57 / / SYM eurjchem-29 1 58 eurjchem.1.3.168‐172.29 eurjchem.1.3.168‐172.29 NOUN eurjchem-29 1 59                 SPACE eurjchem-29 1 60 european european ADJ eurjchem-29 1 61     SPACE eurjchem-29 1 62 journal journal NOUN eurjchem-29 1 63     SPACE eurjchem-29 1 64 of of ADP eurjchem-29 1 65     SPACE eurjchem-29 1 66 chemistry chemistry NOUN eurjchem-29 1 67     SPACE eurjchem-29 1 68 journal journal NOUN eurjchem-29 1 69     SPACE eurjchem-29 1 70 homepage homepage NOUN eurjchem-29 1 71 : : PUNCT eurjchem-29 1 72     SPACE eurjchem-29 1 73 www.eurjchem.com www.eurjchem.com NOUN eurjchem-29 1 74                     SPACE eurjchem-29 1 75 synthesis synthesis NOUN eurjchem-29 1 76     SPACE eurjchem-29 1 77 and and CCONJ eurjchem-29 1 78     SPACE eurjchem-29 1 79 antimicrobial antimicrobial ADJ eurjchem-29 1 80     SPACE eurjchem-29 1 81 evaluation evaluation NOUN eurjchem-29 1 82     SPACE eurjchem-29 1 83 of of ADP eurjchem-29 1 84     SPACE eurjchem-29 1 85 some some DET eurjchem-29 1 86     SPACE eurjchem-29 1 87 new new ADJ eurjchem-29 1 88     SPACE eurjchem-29 1 89 polyheterocyclic polyheterocyclic NOUN eurjchem-29 1 90     SPACE eurjchem-29 1 91 systems system NOUN eurjchem-29 1 92     SPACE eurjchem-29 1 93 containing contain VERB eurjchem-29 1 94     SPACE eurjchem-29 1 95 1,2,4‐triazine 1,2,4‐triazine NUM eurjchem-29 1 96     SPACE eurjchem-29 1 97 moiety moiety NOUN eurjchem-29 1 98     SPACE eurjchem-29 1 99 wafaa wafaa PROPN eurjchem-29 1 100     SPACE eurjchem-29 1 101 ramzy ramzy PROPN eurjchem-29 1 102     SPACE eurjchem-29 1 103 abdel‐monem abdel‐monem PROPN eurjchem-29 1 104     SPACE eurjchem-29 1 105 department department NOUN eurjchem-29 1 106     SPACE eurjchem-29 1 107 of of ADP eurjchem-29 1 108     SPACE eurjchem-29 1 109 chemistry chemistry NOUN eurjchem-29 1 110 , , PUNCT eurjchem-29 1 111     SPACE eurjchem-29 1 112 faculty faculty NOUN eurjchem-29 1 113     SPACE eurjchem-29 1 114 of of ADP eurjchem-29 1 115     SPACE eurjchem-29 1 116 education education NOUN eurjchem-29 1 117 , , PUNCT eurjchem-29 1 118     SPACE eurjchem-29 1 119 ain­shams ain­shams NOUN eurjchem-29 1 120     SPACE eurjchem-29 1 121 university university NOUN eurjchem-29 1 122 , , PUNCT eurjchem-29 1 123     SPACE eurjchem-29 1 124 roxy roxy PROPN eurjchem-29 1 125 , , PUNCT eurjchem-29 1 126     SPACE eurjchem-29 1 127 cairo cairo PROPN eurjchem-29 1 128 , , PUNCT eurjchem-29 1 129     SPACE eurjchem-29 1 130 11711 11711 NUM eurjchem-29 1 131 , , PUNCT eurjchem-29 1 132     SPACE eurjchem-29 1 133 egypt egypt PROPN eurjchem-29 1 134     SPACE eurjchem-29 1 135 * * PROPN eurjchem-29 1 136 corresponding corresponding ADJ eurjchem-29 1 137     SPACE eurjchem-29 1 138 author author NOUN eurjchem-29 1 139     SPACE eurjchem-29 1 140 at at ADP eurjchem-29 1 141 : : PUNCT eurjchem-29 1 142     SPACE eurjchem-29 1 143 department department NOUN eurjchem-29 1 144     SPACE eurjchem-29 1 145 of of ADP eurjchem-29 1 146     SPACE eurjchem-29 1 147 chemistry chemistry NOUN eurjchem-29 1 148 , , PUNCT eurjchem-29 1 149     SPACE eurjchem-29 1 150 faculty faculty NOUN eurjchem-29 1 151     SPACE eurjchem-29 1 152 of of ADP eurjchem-29 1 153     SPACE eurjchem-29 1 154 education education NOUN eurjchem-29 1 155 , , PUNCT eurjchem-29 1 156     SPACE eurjchem-29 1 157 ain­shams ain­shams NOUN eurjchem-29 1 158     SPACE eurjchem-29 1 159 university university NOUN eurjchem-29 1 160 , , PUNCT eurjchem-29 1 161     SPACE eurjchem-29 1 162 roxy roxy PROPN eurjchem-29 1 163 , , PUNCT eurjchem-29 1 164     SPACE eurjchem-29 1 165 cairo cairo PROPN eurjchem-29 1 166 , , PUNCT eurjchem-29 1 167     SPACE eurjchem-29 1 168 11711 11711 NUM eurjchem-29 1 169 , , PUNCT eurjchem-29 1 170     SPACE eurjchem-29 1 171 egypt egypt PROPN eurjchem-29 1 172 . . PUNCT eurjchem-29 1 173     SPACE eurjchem-29 2 1 tel tel PROPN eurjchem-29 2 2 . . PUNCT eurjchem-29 2 3 : : PUNCT eurjchem-29 2 4     SPACE eurjchem-29 2 5 +20125905267 +20125905267 NOUN eurjchem-29 2 6 ; ; PUNCT eurjchem-29 2 7     SPACE eurjchem-29 2 8 fax fax NOUN eurjchem-29 2 9 : : PUNCT eurjchem-29 2 10     SPACE eurjchem-29 2 11 +2026384802 +2026384802 ADJ eurjchem-29 2 12 . . PUNCT eurjchem-29 2 13     SPACE eurjchem-29 2 14 e­mail e­mail NOUN eurjchem-29 2 15     SPACE eurjchem-29 2 16 address address NOUN eurjchem-29 2 17 : : PUNCT eurjchem-29 2 18     SPACE eurjchem-29 3 1 wafaar@hotmail.com wafaar@hotmail.com PROPN eurjchem-29 3 2       SPACE eurjchem-29 3 3 ( ( PUNCT eurjchem-29 3 4 w.r w.r PROPN eurjchem-29 3 5 . . PROPN eurjchem-29 3 6     SPACE eurjchem-29 3 7 abdel­monem abdel­monem NOUN eurjchem-29 3 8 ) ) PUNCT eurjchem-29 3 9 . . PUNCT eurjchem-29 3 10                                 SPACE eurjchem-29 4 1 article article NOUN eurjchem-29 4 2     SPACE eurjchem-29 4 3 information information NOUN eurjchem-29 4 4         SPACE eurjchem-29 4 5 abstract abstract ADJ eurjchem-29 4 6 received receive VERB eurjchem-29 4 7 : : PUNCT eurjchem-29 4 8     SPACE eurjchem-29 4 9 1 1 NUM eurjchem-29 4 10     SPACE eurjchem-29 4 11 april april PROPN eurjchem-29 4 12     SPACE eurjchem-29 4 13 2010 2010 NUM eurjchem-29 4 14     SPACE eurjchem-29 4 15 received receive VERB eurjchem-29 4 16     SPACE eurjchem-29 4 17 in in ADP eurjchem-29 4 18     SPACE eurjchem-29 4 19 revised revise VERB eurjchem-29 4 20     SPACE eurjchem-29 4 21 form form NOUN eurjchem-29 4 22 : : PUNCT eurjchem-29 4 23     SPACE eurjchem-29 4 24 11 11 NUM eurjchem-29 4 25     SPACE eurjchem-29 4 26 june june PROPN eurjchem-29 4 27     SPACE eurjchem-29 4 28 2010 2010 NUM eurjchem-29 4 29     SPACE eurjchem-29 4 30 accepted accept VERB eurjchem-29 4 31 : : PUNCT eurjchem-29 4 32     SPACE eurjchem-29 4 33 15 15 NUM eurjchem-29 4 34     SPACE eurjchem-29 4 35 july july PROPN eurjchem-29 4 36     SPACE eurjchem-29 4 37 2010 2010 NUM eurjchem-29 4 38     SPACE eurjchem-29 4 39 online online NOUN eurjchem-29 4 40 : : PUNCT eurjchem-29 4 41     SPACE eurjchem-29 4 42 30 30 NUM eurjchem-29 4 43     SPACE eurjchem-29 4 44 september september PROPN eurjchem-29 4 45       SPACE eurjchem-29 4 46 2010 2010 NUM eurjchem-29 4 47     SPACE eurjchem-29 4 48 keywords keyword VERB eurjchem-29 4 49         SPACE eurjchem-29 4 50 7‐(4‐chloro/3‐nitrophenyl)‐8‐[5,6‐diphenyl‐4‐(1,3‐thiazol‐2‐yl)‐1,4‐dihydro‐1,2,4‐triazin‐3‐ 7‐(4‐chloro/3‐nitrophenyl)‐8‐[5,6‐diphenyl‐4‐(1,3‐thiazol‐2‐yl)‐1,4‐dihydro‐1,2,4‐triazin‐3‐ NUM eurjchem-29 4 51 yl]‐5‐oxo‐1,5‐dihydro[1,2,4]triazolo[1,5‐a]pyridine‐6‐carbonitrile yl]‐5‐oxo‐1,5‐dihydro[1,2,4]triazolo[1,5‐a]pyridine‐6‐carbonitrile NOUN eurjchem-29 4 52     SPACE eurjchem-29 4 53 ( ( PUNCT eurjchem-29 4 54 6a 6a NOUN eurjchem-29 4 55 , , PUNCT eurjchem-29 4 56     SPACE eurjchem-29 4 57 b b NOUN eurjchem-29 4 58 ) ) PUNCT eurjchem-29 4 59     SPACE eurjchem-29 4 60 was be AUX eurjchem-29 4 61     SPACE eurjchem-29 4 62 utilized utilize VERB eurjchem-29 4 63     SPACE eurjchem-29 4 64 as as ADP eurjchem-29 4 65     SPACE eurjchem-29 4 66 a a DET eurjchem-29 4 67     SPACE eurjchem-29 4 68 key key ADJ eurjchem-29 4 69     SPACE eurjchem-29 4 70 intermediate intermediate ADJ eurjchem-29 4 71     SPACE eurjchem-29 4 72 for for ADP eurjchem-29 4 73     SPACE eurjchem-29 4 74 the the DET eurjchem-29 4 75     SPACE eurjchem-29 4 76 target target NOUN eurjchem-29 4 77     SPACE eurjchem-29 4 78 polyheterocyclic polyheterocyclic NOUN eurjchem-29 4 79     SPACE eurjchem-29 4 80 systems system NOUN eurjchem-29 4 81 . . PUNCT eurjchem-29 4 82     SPACE eurjchem-29 5 1 reactions reaction NOUN eurjchem-29 5 2     SPACE eurjchem-29 5 3 of of ADP eurjchem-29 5 4     SPACE eurjchem-29 5 5 6a 6a NOUN eurjchem-29 5 6 , , PUNCT eurjchem-29 5 7     SPACE eurjchem-29 5 8 b b NOUN eurjchem-29 5 9     SPACE eurjchem-29 5 10 with with ADP eurjchem-29 5 11     SPACE eurjchem-29 5 12 halocarbonyl halocarbonyl ADJ eurjchem-29 5 13     SPACE eurjchem-29 5 14 reagents reagent NOUN eurjchem-29 5 15     SPACE eurjchem-29 5 16 followed follow VERB eurjchem-29 5 17     SPACE eurjchem-29 5 18 by by ADP eurjchem-29 5 19     SPACE eurjchem-29 5 20 heterocyclization heterocyclization NOUN eurjchem-29 5 21     SPACE eurjchem-29 5 22 with with ADP eurjchem-29 5 23     SPACE eurjchem-29 5 24 bi‐nitrogen bi‐nitrogen PROPN eurjchem-29 5 25     SPACE eurjchem-29 5 26 nucleophiles nucleophile NOUN eurjchem-29 5 27     SPACE eurjchem-29 5 28 gave give VERB eurjchem-29 5 29     SPACE eurjchem-29 5 30 some some DET eurjchem-29 5 31     SPACE eurjchem-29 5 32 new new ADJ eurjchem-29 5 33     SPACE eurjchem-29 5 34 nitrogen nitrogen NOUN eurjchem-29 5 35     SPACE eurjchem-29 5 36 heterocycles heterocycle NOUN eurjchem-29 5 37     SPACE eurjchem-29 5 38 ( ( PUNCT eurjchem-29 5 39 7‐13 7‐13 NUM eurjchem-29 5 40 ) ) PUNCT eurjchem-29 5 41 . . PUNCT eurjchem-29 5 42     SPACE eurjchem-29 6 1 structures structure NOUN eurjchem-29 6 2     SPACE eurjchem-29 6 3 of of ADP eurjchem-29 6 4     SPACE eurjchem-29 6 5 the the DET eurjchem-29 6 6     SPACE eurjchem-29 6 7 new new ADJ eurjchem-29 6 8     SPACE eurjchem-29 6 9 compounds compound NOUN eurjchem-29 6 10     SPACE eurjchem-29 6 11 were be AUX eurjchem-29 6 12     SPACE eurjchem-29 6 13 established establish VERB eurjchem-29 6 14     SPACE eurjchem-29 6 15 by by ADP eurjchem-29 6 16     SPACE eurjchem-29 6 17 elemental elemental NOUN eurjchem-29 6 18     SPACE eurjchem-29 6 19 analyses analysis NOUN eurjchem-29 6 20     SPACE eurjchem-29 6 21 and and CCONJ eurjchem-29 6 22     SPACE eurjchem-29 6 23 spectral spectral ADJ eurjchem-29 6 24     SPACE eurjchem-29 6 25 data datum NOUN eurjchem-29 6 26 . . PUNCT eurjchem-29 6 27     SPACE eurjchem-29 7 1 the the DET eurjchem-29 7 2     SPACE eurjchem-29 7 3 synthesized synthesize VERB eurjchem-29 7 4     SPACE eurjchem-29 7 5 compounds compound NOUN eurjchem-29 7 6     SPACE eurjchem-29 7 7 were be AUX eurjchem-29 7 8     SPACE eurjchem-29 7 9 screened screen VERB eurjchem-29 7 10     SPACE eurjchem-29 7 11 for for ADP eurjchem-29 7 12     SPACE eurjchem-29 7 13 their their PRON eurjchem-29 7 14     SPACE eurjchem-29 7 15 antimicrobial antimicrobial ADJ eurjchem-29 7 16     SPACE eurjchem-29 7 17 activity activity NOUN eurjchem-29 7 18 . . PUNCT eurjchem-29 7 19     SPACE eurjchem-29 7 20 1,2,4‐triazine 1,2,4‐triazine NUM eurjchem-29 7 21     SPACE eurjchem-29 7 22 1,2,4‐triazole 1,2,4‐triazole NUM eurjchem-29 7 23     SPACE eurjchem-29 7 24 imidazole imidazole NOUN eurjchem-29 7 25     SPACE eurjchem-29 7 26 polyheterocyclic polyheterocyclic NOUN eurjchem-29 7 27     SPACE eurjchem-29 7 28 nitrogen nitrogen NOUN eurjchem-29 7 29     SPACE eurjchem-29 7 30 systems system NOUN eurjchem-29 7 31     SPACE eurjchem-29 7 32 antimicrobial antimicrobial ADJ eurjchem-29 7 33     SPACE eurjchem-29 7 34 activity activity NOUN eurjchem-29 7 35         SPACE eurjchem-29 7 36 1 1 NUM eurjchem-29 7 37 . . PUNCT eurjchem-29 7 38     SPACE eurjchem-29 7 39 introduction introduction NOUN eurjchem-29 7 40         SPACE eurjchem-29 7 41 1,2,4‐triazines 1,2,4‐triazine NOUN eurjchem-29 7 42     SPACE eurjchem-29 7 43 and and CCONJ eurjchem-29 7 44     SPACE eurjchem-29 7 45 their their PRON eurjchem-29 7 46     SPACE eurjchem-29 7 47 derivatives derivative NOUN eurjchem-29 7 48     SPACE eurjchem-29 7 49 occupy occupy VERB eurjchem-29 7 50     SPACE eurjchem-29 7 51 a a DET eurjchem-29 7 52     SPACE eurjchem-29 7 53 pivotal pivotal ADJ eurjchem-29 7 54     SPACE eurjchem-29 7 55 position position NOUN eurjchem-29 7 56     SPACE eurjchem-29 7 57 in in ADP eurjchem-29 7 58     SPACE eurjchem-29 7 59 modern modern ADJ eurjchem-29 7 60     SPACE eurjchem-29 7 61 medicinal medicinal ADJ eurjchem-29 7 62     SPACE eurjchem-29 7 63 chemistry chemistry NOUN eurjchem-29 7 64 , , PUNCT eurjchem-29 7 65     SPACE eurjchem-29 7 66 because because SCONJ eurjchem-29 7 67     SPACE eurjchem-29 7 68 of of ADP eurjchem-29 7 69     SPACE eurjchem-29 7 70 their their PRON eurjchem-29 7 71     SPACE eurjchem-29 7 72 high high ADJ eurjchem-29 7 73     SPACE eurjchem-29 7 74 potential potential NOUN eurjchem-29 7 75     SPACE eurjchem-29 7 76 for for ADP eurjchem-29 7 77     SPACE eurjchem-29 7 78 biological biological ADJ eurjchem-29 7 79     SPACE eurjchem-29 7 80 activity activity NOUN eurjchem-29 7 81 . . PUNCT eurjchem-29 7 82     SPACE eurjchem-29 7 83 various various ADJ eurjchem-29 7 84     SPACE eurjchem-29 7 85 1,2,4‐triazine 1,2,4‐triazine NUM eurjchem-29 7 86     SPACE eurjchem-29 7 87 derivatives derivative NOUN eurjchem-29 7 88     SPACE eurjchem-29 7 89 found find VERB eurjchem-29 7 90     SPACE eurjchem-29 7 91 application application NOUN eurjchem-29 7 92     SPACE eurjchem-29 7 93 as as ADP eurjchem-29 7 94     SPACE eurjchem-29 7 95 pharmaceuticals pharmaceutical NOUN eurjchem-29 7 96 , , PUNCT eurjchem-29 7 97     SPACE eurjchem-29 7 98 herbicides herbicide NOUN eurjchem-29 7 99 , , PUNCT eurjchem-29 7 100     SPACE eurjchem-29 7 101 pesticides pesticide NOUN eurjchem-29 7 102     SPACE eurjchem-29 7 103 and and CCONJ eurjchem-29 7 104     SPACE eurjchem-29 7 105 dyes dye NOUN eurjchem-29 7 106     SPACE eurjchem-29 8 1 [ [ X eurjchem-29 8 2 1‐5 1‐5 NUM eurjchem-29 8 3 ] ] X eurjchem-29 8 4 . . PUNCT eurjchem-29 8 5     SPACE eurjchem-29 9 1 moreover moreover ADV eurjchem-29 9 2 , , PUNCT eurjchem-29 9 3     SPACE eurjchem-29 9 4 in in ADP eurjchem-29 9 5     SPACE eurjchem-29 9 6 recent recent ADJ eurjchem-29 9 7     SPACE eurjchem-29 9 8 years year NOUN eurjchem-29 9 9 , , PUNCT eurjchem-29 9 10     SPACE eurjchem-29 9 11 1,2,4‐ 1,2,4‐ NUM eurjchem-29 9 12 triazine triazine NOUN eurjchem-29 9 13     SPACE eurjchem-29 9 14 compounds compound NOUN eurjchem-29 9 15     SPACE eurjchem-29 9 16 have have AUX eurjchem-29 9 17     SPACE eurjchem-29 9 18 been be AUX eurjchem-29 9 19     SPACE eurjchem-29 9 20 reported report VERB eurjchem-29 9 21     SPACE eurjchem-29 9 22 to to PART eurjchem-29 9 23     SPACE eurjchem-29 9 24 possess possess VERB eurjchem-29 9 25     SPACE eurjchem-29 9 26 biological biological ADJ eurjchem-29 9 27     SPACE eurjchem-29 9 28 activities activity NOUN eurjchem-29 9 29     SPACE eurjchem-29 9 30 as as ADV eurjchem-29 9 31     SPACE eurjchem-29 9 32 anti‐aids anti‐aid NOUN eurjchem-29 9 33     SPACE eurjchem-29 9 34 [ [ X eurjchem-29 9 35 6 6 NUM eurjchem-29 9 36 ] ] PUNCT eurjchem-29 9 37 , , PUNCT eurjchem-29 9 38         SPACE eurjchem-29 9 39 anticancer anticancer NOUN eurjchem-29 9 40     SPACE eurjchem-29 10 1 [ [ X eurjchem-29 10 2 7 7 NUM eurjchem-29 10 3 ] ] PUNCT eurjchem-29 10 4 , , PUNCT eurjchem-29 10 5     SPACE eurjchem-29 10 6 anti‐inflammatory anti‐inflammatory NOUN eurjchem-29 10 7     SPACE eurjchem-29 11 1 [ [ X eurjchem-29 11 2 8 8 NUM eurjchem-29 11 3 ] ] PUNCT eurjchem-29 11 4 , , PUNCT eurjchem-29 11 5     SPACE eurjchem-29 11 6 antihypertensive antihypertensive ADJ eurjchem-29 11 7     SPACE eurjchem-29 11 8 activities activity NOUN eurjchem-29 11 9     SPACE eurjchem-29 12 1 [ [ X eurjchem-29 12 2 9 9 NUM eurjchem-29 12 3 ] ] PUNCT eurjchem-29 12 4     SPACE eurjchem-29 12 5 and and CCONJ eurjchem-29 12 6     SPACE eurjchem-29 12 7 antimicrobial antimicrobial ADJ eurjchem-29 12 8     SPACE eurjchem-29 12 9 activities activity NOUN eurjchem-29 12 10     SPACE eurjchem-29 12 11 [ [ X eurjchem-29 12 12 10‐11 10‐11 NUM eurjchem-29 12 13 ] ] PUNCT eurjchem-29 12 14 . . PUNCT eurjchem-29 12 15     SPACE eurjchem-29 12 16 prompted prompt VERB eurjchem-29 12 17     SPACE eurjchem-29 12 18 by by ADP eurjchem-29 12 19     SPACE eurjchem-29 12 20 the the DET eurjchem-29 12 21     SPACE eurjchem-29 12 22 varied varied ADJ eurjchem-29 12 23     SPACE eurjchem-29 12 24 biological biological ADJ eurjchem-29 12 25     SPACE eurjchem-29 12 26 activities activity NOUN eurjchem-29 12 27     SPACE eurjchem-29 12 28 of of ADP eurjchem-29 12 29     SPACE eurjchem-29 12 30 1,2,4‐ 1,2,4‐ NUM eurjchem-29 12 31 triazole triazole NOUN eurjchem-29 12 32     SPACE eurjchem-29 12 33 moieties moiety NOUN eurjchem-29 12 34     SPACE eurjchem-29 13 1 [ [ X eurjchem-29 13 2 12‐13 12‐13 NUM eurjchem-29 13 3 ] ] X eurjchem-29 13 4     SPACE eurjchem-29 13 5 that that PRON eurjchem-29 13 6     SPACE eurjchem-29 13 7 are be AUX eurjchem-29 13 8     SPACE eurjchem-29 13 9 bearing bear VERB eurjchem-29 13 10     SPACE eurjchem-29 13 11 nitrogen nitrogen NOUN eurjchem-29 13 12     SPACE eurjchem-29 13 13 heterocyclic heterocyclic ADJ eurjchem-29 13 14     SPACE eurjchem-29 13 15 system system NOUN eurjchem-29 13 16     SPACE eurjchem-29 13 17 to to PART eurjchem-29 13 18     SPACE eurjchem-29 13 19 study study VERB eurjchem-29 13 20     SPACE eurjchem-29 13 21 the the DET eurjchem-29 13 22     SPACE eurjchem-29 13 23 biological biological ADJ eurjchem-29 13 24     SPACE eurjchem-29 13 25 activity activity NOUN eurjchem-29 13 26 . . PUNCT eurjchem-29 13 27     SPACE eurjchem-29 14 1 derivatives derivative NOUN eurjchem-29 14 2     SPACE eurjchem-29 14 3 of of ADP eurjchem-29 14 4     SPACE eurjchem-29 14 5 some some DET eurjchem-29 14 6     SPACE eurjchem-29 14 7 new new ADJ eurjchem-29 14 8     SPACE eurjchem-29 14 9 1,2,4‐triazines 1,2,4‐triazine NOUN eurjchem-29 14 10     SPACE eurjchem-29 14 11 bearing bear VERB eurjchem-29 14 12     SPACE eurjchem-29 14 13 nitrogen nitrogen NOUN eurjchem-29 14 14     SPACE eurjchem-29 14 15 heterocyclic heterocyclic NOUN eurjchem-29 14 16     SPACE eurjchem-29 14 17 systems system NOUN eurjchem-29 14 18     SPACE eurjchem-29 14 19 are be AUX eurjchem-29 14 20     SPACE eurjchem-29 14 21 generally generally ADV eurjchem-29 14 22     SPACE eurjchem-29 14 23 prepared prepare VERB eurjchem-29 14 24     SPACE eurjchem-29 14 25 from from ADP eurjchem-29 14 26     SPACE eurjchem-29 14 27 1,2‐diamino 1,2‐diamino NOUN eurjchem-29 14 28     SPACE eurjchem-29 14 29 pyridines pyridine NOUN eurjchem-29 14 30     SPACE eurjchem-29 15 1 [ [ X eurjchem-29 15 2 14‐15 14‐15 NUM eurjchem-29 15 3 ] ] PUNCT eurjchem-29 15 4 . . PUNCT eurjchem-29 15 5     SPACE eurjchem-29 16 1 in in ADP eurjchem-29 16 2     SPACE eurjchem-29 16 3 continuation continuation NOUN eurjchem-29 16 4     SPACE eurjchem-29 16 5 of of ADP eurjchem-29 16 6     SPACE eurjchem-29 16 7 our our PRON eurjchem-29 16 8     SPACE eurjchem-29 16 9 work work NOUN eurjchem-29 16 10     SPACE eurjchem-29 16 11 in in ADP eurjchem-29 16 12     SPACE eurjchem-29 16 13 the the DET eurjchem-29 16 14     SPACE eurjchem-29 16 15 area area NOUN eurjchem-29 16 16     SPACE eurjchem-29 16 17 of of ADP eurjchem-29 16 18     SPACE eurjchem-29 16 19 1,2,4‐triazine 1,2,4‐triazine NUM eurjchem-29 16 20     SPACE eurjchem-29 16 21 chemistry chemistry NOUN eurjchem-29 16 22     SPACE eurjchem-29 17 1 [ [ X eurjchem-29 17 2 16‐19 16‐19 NUM eurjchem-29 17 3 ] ] PUNCT eurjchem-29 17 4     SPACE eurjchem-29 17 5 and and CCONJ eurjchem-29 17 6     SPACE eurjchem-29 17 7 their their PRON eurjchem-29 17 8     SPACE eurjchem-29 17 9 heterocyclization heterocyclization NOUN eurjchem-29 17 10     SPACE eurjchem-29 17 11 via via ADP eurjchem-29 17 12     SPACE eurjchem-29 17 13 ring ring NOUN eurjchem-29 17 14     SPACE eurjchem-29 17 15 closure closure NOUN eurjchem-29 17 16     SPACE eurjchem-29 17 17 reactions reaction NOUN eurjchem-29 17 18     SPACE eurjchem-29 17 19 with with ADP eurjchem-29 17 20     SPACE eurjchem-29 17 21 halocarbonyl halocarbonyl ADJ eurjchem-29 17 22     SPACE eurjchem-29 17 23 reagents reagent NOUN eurjchem-29 17 24 , , PUNCT eurjchem-29 17 25     SPACE eurjchem-29 17 26 the the DET eurjchem-29 17 27     SPACE eurjchem-29 17 28 present present ADJ eurjchem-29 17 29     SPACE eurjchem-29 17 30 work work NOUN eurjchem-29 17 31     SPACE eurjchem-29 17 32 aimed aim VERB eurjchem-29 17 33     SPACE eurjchem-29 17 34 to to PART eurjchem-29 17 35     SPACE eurjchem-29 17 36 synthesize synthesize VERB eurjchem-29 17 37     SPACE eurjchem-29 17 38 of of ADP eurjchem-29 17 39     SPACE eurjchem-29 17 40 some some DET eurjchem-29 17 41     SPACE eurjchem-29 17 42 new new ADJ eurjchem-29 17 43     SPACE eurjchem-29 17 44 1,2,4‐triazines 1,2,4‐triazine NOUN eurjchem-29 17 45     SPACE eurjchem-29 17 46 bearing bear VERB eurjchem-29 17 47     SPACE eurjchem-29 17 48 nitrogen nitrogen NOUN eurjchem-29 17 49     SPACE eurjchem-29 17 50 heterocyclic heterocyclic NOUN eurjchem-29 17 51     SPACE eurjchem-29 17 52 systems system NOUN eurjchem-29 17 53 , , PUNCT eurjchem-29 17 54     SPACE eurjchem-29 17 55 as as ADV eurjchem-29 17 56     SPACE eurjchem-29 17 57 well well ADV eurjchem-29 17 58     SPACE eurjchem-29 17 59 as as SCONJ eurjchem-29 17 60     SPACE eurjchem-29 17 61 their their PRON eurjchem-29 17 62     SPACE eurjchem-29 17 63 antimicrobial antimicrobial ADJ eurjchem-29 17 64     SPACE eurjchem-29 17 65 activity activity NOUN eurjchem-29 17 66     SPACE eurjchem-29 17 67 were be AUX eurjchem-29 17 68     SPACE eurjchem-29 17 69 screened screen VERB eurjchem-29 17 70 . . PUNCT eurjchem-29 17 71           SPACE eurjchem-29 18 1 2 2 NUM eurjchem-29 18 2 . . PUNCT eurjchem-29 18 3     SPACE eurjchem-29 18 4 experimental experimental ADJ eurjchem-29 18 5         SPACE eurjchem-29 18 6 2.1 2.1 NUM eurjchem-29 18 7 . . PUNCT eurjchem-29 18 8     SPACE eurjchem-29 18 9 instrumentation instrumentation NOUN eurjchem-29 18 10         SPACE eurjchem-29 18 11 melting melting NOUN eurjchem-29 18 12     SPACE eurjchem-29 18 13 points point NOUN eurjchem-29 18 14     SPACE eurjchem-29 18 15 were be AUX eurjchem-29 18 16     SPACE eurjchem-29 18 17 determined determine VERB eurjchem-29 18 18     SPACE eurjchem-29 18 19 on on ADP eurjchem-29 18 20     SPACE eurjchem-29 18 21 a a DET eurjchem-29 18 22     SPACE eurjchem-29 18 23 digital digital ADJ eurjchem-29 18 24     SPACE eurjchem-29 18 25 stuart stuart PROPN eurjchem-29 18 26     SPACE eurjchem-29 18 27 smp‐3 smp‐3 PROPN eurjchem-29 18 28     SPACE eurjchem-29 18 29 apparatus apparatus NOUN eurjchem-29 18 30 . . PUNCT eurjchem-29 18 31     SPACE eurjchem-29 19 1 infrared infrare VERB eurjchem-29 19 2     SPACE eurjchem-29 19 3 spectra spectra PROPN eurjchem-29 19 4     SPACE eurjchem-29 19 5 were be AUX eurjchem-29 19 6     SPACE eurjchem-29 19 7 recorded record VERB eurjchem-29 19 8     SPACE eurjchem-29 19 9 on on ADP eurjchem-29 19 10     SPACE eurjchem-29 19 11 ft‐ir ft‐ir NOUN eurjchem-29 19 12     SPACE eurjchem-29 19 13 bruker bruker NOUN eurjchem-29 19 14     SPACE eurjchem-29 19 15 vector vector NOUN eurjchem-29 19 16     SPACE eurjchem-29 19 17 22 22 NUM eurjchem-29 19 18     SPACE eurjchem-29 19 19 spectrophotometer spectrophotometer NOUN eurjchem-29 19 20     SPACE eurjchem-29 19 21 using use VERB eurjchem-29 19 22     SPACE eurjchem-29 19 23 kbr kbr PROPN eurjchem-29 19 24     SPACE eurjchem-29 19 25 wafer wafer NOUN eurjchem-29 19 26     SPACE eurjchem-29 19 27 technique technique NOUN eurjchem-29 19 28 . . PUNCT eurjchem-29 19 29     SPACE eurjchem-29 19 30 1h 1h NUM eurjchem-29 19 31     SPACE eurjchem-29 19 32 nmr nmr NOUN eurjchem-29 19 33     SPACE eurjchem-29 19 34 spectra spectra NOUN eurjchem-29 19 35     SPACE eurjchem-29 19 36 were be AUX eurjchem-29 19 37     SPACE eurjchem-29 19 38 measured measure VERB eurjchem-29 19 39     SPACE eurjchem-29 19 40 on on ADP eurjchem-29 19 41     SPACE eurjchem-29 19 42 gemini gemini NOUN eurjchem-29 19 43     SPACE eurjchem-29 19 44 spectrometer spectrometer NOUN eurjchem-29 19 45     SPACE eurjchem-29 19 46 200 200 NUM eurjchem-29 19 47     SPACE eurjchem-29 19 48 mhz mhz NOUN eurjchem-29 19 49     SPACE eurjchem-29 19 50 using use VERB eurjchem-29 19 51     SPACE eurjchem-29 19 52 dmso‐d6 dmso‐d6 NOUN eurjchem-29 19 53     SPACE eurjchem-29 19 54 as as ADP eurjchem-29 19 55     SPACE eurjchem-29 19 56 solvent solvent NOUN eurjchem-29 19 57     SPACE eurjchem-29 19 58 and and CCONJ eurjchem-29 19 59     SPACE eurjchem-29 19 60 tms tms PROPN eurjchem-29 19 61     SPACE eurjchem-29 19 62 ( ( PUNCT eurjchem-29 19 63 chemical chemical NOUN eurjchem-29 19 64     SPACE eurjchem-29 19 65 sift sift NOUN eurjchem-29 19 66     SPACE eurjchem-29 19 67 in in ADP eurjchem-29 19 68     SPACE eurjchem-29 19 69 δ δ PROPN eurjchem-29 19 70     SPACE eurjchem-29 19 71 ppm ppm NOUN eurjchem-29 19 72 ) ) PUNCT eurjchem-29 19 73     SPACE eurjchem-29 19 74 as as ADP eurjchem-29 19 75     SPACE eurjchem-29 19 76 an an DET eurjchem-29 19 77     SPACE eurjchem-29 19 78 internal internal ADJ eurjchem-29 19 79     SPACE eurjchem-29 19 80 standard standard NOUN eurjchem-29 19 81 . . PUNCT eurjchem-29 19 82     SPACE eurjchem-29 19 83 mass mass PROPN eurjchem-29 19 84     SPACE eurjchem-29 19 85 spectra spectra NOUN eurjchem-29 19 86     SPACE eurjchem-29 19 87 were be AUX eurjchem-29 19 88     SPACE eurjchem-29 19 89 obtained obtain VERB eurjchem-29 19 90     SPACE eurjchem-29 19 91 through through ADP eurjchem-29 19 92     SPACE eurjchem-29 19 93 gcms gcms NOUN eurjchem-29 19 94     SPACE eurjchem-29 19 95 qp qp ADP eurjchem-29 19 96     SPACE eurjchem-29 19 97 1000 1000 NUM eurjchem-29 19 98     SPACE eurjchem-29 19 99 ex ex NOUN eurjchem-29 19 100     SPACE eurjchem-29 19 101 schimadzu schimadzu NOUN eurjchem-29 19 102     SPACE eurjchem-29 19 103 instrument instrument NOUN eurjchem-29 19 104     SPACE eurjchem-29 19 105 mass mass PROPN eurjchem-29 19 106     SPACE eurjchem-29 19 107 spectrometer spectrometer NOUN eurjchem-29 19 108     SPACE eurjchem-29 19 109 ( ( PUNCT eurjchem-29 19 110 70 70 NUM eurjchem-29 19 111     SPACE eurjchem-29 19 112 ev ev NOUN eurjchem-29 19 113 ) ) PUNCT eurjchem-29 19 114 . . PUNCT eurjchem-29 19 115     SPACE eurjchem-29 20 1 elemental elemental NOUN eurjchem-29 20 2     SPACE eurjchem-29 20 3 micro‐analyses micro‐analyse NOUN eurjchem-29 20 4     SPACE eurjchem-29 20 5 were be AUX eurjchem-29 20 6     SPACE eurjchem-29 20 7 performed perform VERB eurjchem-29 20 8     SPACE eurjchem-29 20 9 at at ADP eurjchem-29 20 10     SPACE eurjchem-29 20 11 the the DET eurjchem-29 20 12     SPACE eurjchem-29 20 13 cairo cairo PROPN eurjchem-29 20 14     SPACE eurjchem-29 20 15 university university NOUN eurjchem-29 20 16     SPACE eurjchem-29 20 17 microanalytical microanalytical ADJ eurjchem-29 20 18     SPACE eurjchem-29 20 19 center center NOUN eurjchem-29 20 20 . . PUNCT eurjchem-29 20 21     SPACE eurjchem-29 21 1 the the DET eurjchem-29 21 2     SPACE eurjchem-29 21 3 purity purity NOUN eurjchem-29 21 4     SPACE eurjchem-29 21 5 of of ADP eurjchem-29 21 6     SPACE eurjchem-29 21 7 the the DET eurjchem-29 21 8     SPACE eurjchem-29 21 9 synthesized synthesize VERB eurjchem-29 21 10     SPACE eurjchem-29 21 11 compounds compound NOUN eurjchem-29 21 12     SPACE eurjchem-29 21 13 was be AUX eurjchem-29 21 14     SPACE eurjchem-29 21 15 checked check VERB eurjchem-29 21 16     SPACE eurjchem-29 21 17 by by ADP eurjchem-29 21 18     SPACE eurjchem-29 21 19 thin thin ADJ eurjchem-29 21 20     SPACE eurjchem-29 21 21 layer layer NOUN eurjchem-29 21 22     SPACE eurjchem-29 21 23 chromatography chromatography NOUN eurjchem-29 21 24     SPACE eurjchem-29 21 25 on on ADP eurjchem-29 21 26     SPACE eurjchem-29 21 27 silica silica NOUN eurjchem-29 21 28     SPACE eurjchem-29 21 29 gel gel NOUN eurjchem-29 21 30     SPACE eurjchem-29 21 31 ( ( PUNCT eurjchem-29 21 32 silica silica NOUN eurjchem-29 21 33     SPACE eurjchem-29 21 34 gel gel NOUN eurjchem-29 21 35 , , PUNCT eurjchem-29 21 36     SPACE eurjchem-29 21 37 aluminum aluminum NOUN eurjchem-29 21 38     SPACE eurjchem-29 21 39 sheets sheet NOUN eurjchem-29 21 40     SPACE eurjchem-29 21 41 60 60 NUM eurjchem-29 21 42     SPACE eurjchem-29 21 43 f254 f254 PROPN eurjchem-29 21 44 , , PUNCT eurjchem-29 21 45     SPACE eurjchem-29 21 46 merck merck NOUN eurjchem-29 21 47 ) ) PUNCT eurjchem-29 21 48 . . PUNCT eurjchem-29 21 49     SPACE eurjchem-29 22 1 evaluation evaluation NOUN eurjchem-29 22 2     SPACE eurjchem-29 22 3 of of ADP eurjchem-29 22 4     SPACE eurjchem-29 22 5 antimicrobial antimicrobial ADJ eurjchem-29 22 6     SPACE eurjchem-29 22 7 activities activity NOUN eurjchem-29 22 8     SPACE eurjchem-29 22 9 was be AUX eurjchem-29 22 10     SPACE eurjchem-29 22 11 carried carry VERB eurjchem-29 22 12     SPACE eurjchem-29 22 13 out out ADP eurjchem-29 22 14     SPACE eurjchem-29 22 15 by by ADP eurjchem-29 22 16     SPACE eurjchem-29 22 17 the the DET eurjchem-29 22 18     SPACE eurjchem-29 22 19 faculty faculty NOUN eurjchem-29 22 20     SPACE eurjchem-29 22 21 of of ADP eurjchem-29 22 22     SPACE eurjchem-29 22 23 agriculture agriculture NOUN eurjchem-29 22 24     SPACE eurjchem-29 22 25 for for ADP eurjchem-29 22 26     SPACE eurjchem-29 22 27 girls girl NOUN eurjchem-29 22 28     SPACE eurjchem-29 22 29 al‐azhar al‐azhar PROPN eurjchem-29 22 30     SPACE eurjchem-29 22 31 university university NOUN eurjchem-29 22 32 , , PUNCT eurjchem-29 22 33     SPACE eurjchem-29 22 34 nasr nasr PROPN eurjchem-29 22 35     SPACE eurjchem-29 22 36 city city PROPN eurjchem-29 22 37 , , PUNCT eurjchem-29 22 38     SPACE eurjchem-29 22 39 cairo cairo PROPN eurjchem-29 22 40 , , PUNCT eurjchem-29 22 41     SPACE eurjchem-29 22 42 egypt egypt PROPN eurjchem-29 22 43 . . PUNCT eurjchem-29 22 44     SPACE eurjchem-29 23 1 ethyl ethyl PROPN eurjchem-29 23 2     SPACE eurjchem-29 23 3 1,2‐dimino‐5‐cyano‐4‐(4‐ 1,2‐dimino‐5‐cyano‐4‐(4‐ NUM eurjchem-29 23 4 chloro/3‐nitrophenyl)‐6‐oxo‐1,6‐dihydro‐pyridine‐3‐carboxy‐ chloro/3‐nitrophenyl)‐6‐oxo‐1,6‐dihydro‐pyridine‐3‐carboxy‐ ADJ eurjchem-29 23 5 late late ADJ eurjchem-29 23 6     SPACE eurjchem-29 23 7 ( ( PUNCT eurjchem-29 23 8 2a 2a NUM eurjchem-29 23 9 , , PUNCT eurjchem-29 23 10 b b X eurjchem-29 23 11 ) ) PUNCT eurjchem-29 23 12     SPACE eurjchem-29 23 13 were be AUX eurjchem-29 23 14     SPACE eurjchem-29 23 15 prepared prepare VERB eurjchem-29 23 16     SPACE eurjchem-29 23 17 according accord VERB eurjchem-29 23 18     SPACE eurjchem-29 23 19 to to ADP eurjchem-29 23 20     SPACE eurjchem-29 23 21 the the DET eurjchem-29 23 22     SPACE eurjchem-29 23 23 previous previous ADJ eurjchem-29 23 24     SPACE eurjchem-29 23 25 procedure procedure NOUN eurjchem-29 23 26     SPACE eurjchem-29 24 1 [ [ X eurjchem-29 24 2 20 20 NUM eurjchem-29 24 3 ] ] PUNCT eurjchem-29 24 4 . . PUNCT eurjchem-29 24 5         SPACE eurjchem-29 25 1 2.2 2.2 NUM eurjchem-29 25 2 . . PUNCT eurjchem-29 25 3     SPACE eurjchem-29 25 4 synthesis synthesis NOUN eurjchem-29 25 5         SPACE eurjchem-29 25 6 2.2.1 2.2.1 NUM eurjchem-29 25 7 . . PUNCT eurjchem-29 25 8     SPACE eurjchem-29 25 9 ethyl­7­(4­chloro/3­nitrophenyl)­6­cyano­5­oxo­1,5­ ethyl­7­(4­chloro/3­nitrophenyl)­6­cyano­5­oxo­1,5­ PUNCT eurjchem-29 25 10 dihydro[1,2,4]triazolo[1,5­a]pyridine­8­carboxylate dihydro[1,2,4]triazolo[1,5­a]pyridine­8­carboxylate VERB eurjchem-29 25 11     SPACE eurjchem-29 25 12 ( ( PUNCT eurjchem-29 25 13 3a 3a NUM eurjchem-29 25 14 , , PUNCT eurjchem-29 25 15 b b NOUN eurjchem-29 25 16 ) ) PUNCT eurjchem-29 25 17         SPACE eurjchem-29 25 18 a a DET eurjchem-29 25 19     SPACE eurjchem-29 25 20 mixture mixture NOUN eurjchem-29 25 21     SPACE eurjchem-29 25 22 of of ADP eurjchem-29 25 23     SPACE eurjchem-29 25 24 compounds compound NOUN eurjchem-29 25 25     SPACE eurjchem-29 25 26 2a 2a NUM eurjchem-29 25 27 , , PUNCT eurjchem-29 25 28     SPACE eurjchem-29 25 29 b b NOUN eurjchem-29 25 30     SPACE eurjchem-29 25 31 ( ( PUNCT eurjchem-29 25 32 0.01 0.01 NUM eurjchem-29 25 33     SPACE eurjchem-29 25 34 mol mol NOUN eurjchem-29 25 35 ) ) PUNCT eurjchem-29 25 36     SPACE eurjchem-29 25 37 and and CCONJ eurjchem-29 25 38     SPACE eurjchem-29 25 39 triethyl triethyl NOUN eurjchem-29 25 40     SPACE eurjchem-29 25 41 orthoformate orthoformate VERB eurjchem-29 25 42     SPACE eurjchem-29 25 43 ( ( PUNCT eurjchem-29 25 44 0.02 0.02 NUM eurjchem-29 25 45     SPACE eurjchem-29 25 46 mol mol NOUN eurjchem-29 25 47 ) ) PUNCT eurjchem-29 25 48     SPACE eurjchem-29 25 49 was be AUX eurjchem-29 25 50     SPACE eurjchem-29 25 51 refluxed refluxe VERB eurjchem-29 25 52     SPACE eurjchem-29 25 53 for for ADP eurjchem-29 25 54     SPACE eurjchem-29 25 55 3 3 NUM eurjchem-29 25 56     SPACE eurjchem-29 25 57 h. h. NOUN eurjchem-29 25 58     SPACE eurjchem-29 25 59 the the DET eurjchem-29 25 60     SPACE eurjchem-29 25 61 reaction reaction NOUN eurjchem-29 25 62     SPACE eurjchem-29 25 63 mixture mixture NOUN eurjchem-29 25 64     SPACE eurjchem-29 25 65 was be AUX eurjchem-29 25 66     SPACE eurjchem-29 25 67 cooled cool VERB eurjchem-29 25 68     SPACE eurjchem-29 25 69 and and CCONJ eurjchem-29 25 70     SPACE eurjchem-29 25 71 the the DET eurjchem-29 25 72     SPACE eurjchem-29 25 73 solid solid NOUN eurjchem-29 25 74     SPACE eurjchem-29 25 75 obtained obtain VERB eurjchem-29 25 76     SPACE eurjchem-29 25 77 was be AUX eurjchem-29 25 78     SPACE eurjchem-29 25 79 filtered filter VERB eurjchem-29 25 80     SPACE eurjchem-29 25 81 off off ADP eurjchem-29 25 82     SPACE eurjchem-29 25 83 and and CCONJ eurjchem-29 25 84     SPACE eurjchem-29 25 85 crystallized crystallize VERB eurjchem-29 25 86     SPACE eurjchem-29 25 87 to to PART eurjchem-29 25 88     SPACE eurjchem-29 25 89 give give VERB eurjchem-29 25 90     SPACE eurjchem-29 25 91 compounds compound NOUN eurjchem-29 25 92     SPACE eurjchem-29 25 93 3a 3a NUM eurjchem-29 25 94 , , PUNCT eurjchem-29 25 95     SPACE eurjchem-29 25 96 b b NOUN eurjchem-29 25 97 , , PUNCT eurjchem-29 25 98     SPACE eurjchem-29 25 99 respectively respectively ADV eurjchem-29 25 100     SPACE eurjchem-29 25 101 ( ( PUNCT eurjchem-29 25 102 scheme scheme NOUN eurjchem-29 25 103     SPACE eurjchem-29 25 104 1 1 NUM eurjchem-29 25 105 ) ) PUNCT eurjchem-29 25 106 . . PUNCT eurjchem-29 25 107       SPACE eurjchem-29 26 1 compound compound PROPN eurjchem-29 26 2     SPACE eurjchem-29 26 3 3a 3a NUM eurjchem-29 26 4     SPACE eurjchem-29 26 5 was be AUX eurjchem-29 26 6     SPACE eurjchem-29 26 7 crystallized crystallize VERB eurjchem-29 26 8     SPACE eurjchem-29 26 9 from from ADP eurjchem-29 26 10     SPACE eurjchem-29 26 11 1 1 NUM eurjchem-29 26 12 , , PUNCT eurjchem-29 26 13     SPACE eurjchem-29 26 14 4‐dioxane 4‐dioxane NUM eurjchem-29 26 15 . . PUNCT eurjchem-29 26 16     SPACE eurjchem-29 26 17 yield yield NOUN eurjchem-29 26 18 : : PUNCT eurjchem-29 26 19     SPACE eurjchem-29 26 20 72 72 NUM eurjchem-29 26 21 % % NOUN eurjchem-29 26 22 . . PUNCT eurjchem-29 26 23     SPACE eurjchem-29 27 1 m.p m.p PROPN eurjchem-29 27 2 . . PROPN eurjchem-29 27 3 : : PUNCT eurjchem-29 27 4     SPACE eurjchem-29 27 5 238‐240 238‐240 NUM eurjchem-29 27 6     SPACE eurjchem-29 27 7 ºc ºc PROPN eurjchem-29 27 8 . . PUNCT eurjchem-29 27 9       SPACE eurjchem-29 27 10 ft‐ir ft‐ir NOUN eurjchem-29 27 11     SPACE eurjchem-29 27 12 ( ( PUNCT eurjchem-29 27 13 kbr kbr PROPN eurjchem-29 27 14 ) ) PUNCT eurjchem-29 27 15     SPACE eurjchem-29 27 16 ν ν PROPN eurjchem-29 27 17 , , PUNCT eurjchem-29 27 18     SPACE eurjchem-29 27 19 ( ( PUNCT eurjchem-29 27 20 cm‐1 cm‐1 NOUN eurjchem-29 27 21 ): ): PUNCT eurjchem-29 27 22     SPACE eurjchem-29 27 23 3388 3388 NUM eurjchem-29 27 24     SPACE eurjchem-29 27 25 ( ( PUNCT eurjchem-29 27 26 nh nh NOUN eurjchem-29 27 27 ) ) PUNCT eurjchem-29 27 28 , , PUNCT eurjchem-29 27 29     SPACE eurjchem-29 27 30 2195 2195 NUM eurjchem-29 27 31     SPACE eurjchem-29 27 32 ( ( PUNCT eurjchem-29 27 33 c≡n c≡n PROPN eurjchem-29 27 34 ) ) PUNCT eurjchem-29 27 35 , , PUNCT eurjchem-29 27 36     SPACE eurjchem-29 27 37 1774 1774 NUM eurjchem-29 27 38 , , PUNCT eurjchem-29 27 39     SPACE eurjchem-29 27 40 1688 1688 NUM eurjchem-29 27 41     SPACE eurjchem-29 27 42 ( ( PUNCT eurjchem-29 27 43 2 2 NUM eurjchem-29 27 44     SPACE eurjchem-29 27 45 c c NOUN eurjchem-29 27 46 = = NOUN eurjchem-29 27 47 o o NOUN eurjchem-29 27 48 ) ) PUNCT eurjchem-29 27 49 , , PUNCT eurjchem-29 27 50     SPACE eurjchem-29 27 51 1614 1614 NUM eurjchem-29 27 52     SPACE eurjchem-29 27 53 ( ( PUNCT eurjchem-29 27 54 c c X eurjchem-29 27 55 = = SYM eurjchem-29 27 56 c c NOUN eurjchem-29 27 57 ) ) PUNCT eurjchem-29 27 58 , , PUNCT eurjchem-29 27 59     SPACE eurjchem-29 27 60 1566 1566 NUM eurjchem-29 27 61     SPACE eurjchem-29 27 62 ( ( PUNCT eurjchem-29 27 63 c c NOUN eurjchem-29 27 64 = = SYM eurjchem-29 27 65 n n NUM eurjchem-29 27 66 ) ) PUNCT eurjchem-29 27 67 , , PUNCT eurjchem-29 27 68     SPACE eurjchem-29 27 69 673 673 NUM eurjchem-29 27 70     SPACE eurjchem-29 27 71 ( ( PUNCT eurjchem-29 27 72 c c NOUN eurjchem-29 27 73 – – PUNCT eurjchem-29 27 74 cl cl NOUN eurjchem-29 27 75 ) ) PUNCT eurjchem-29 27 76 . . PUNCT eurjchem-29 27 77     SPACE eurjchem-29 28 1 1h 1h NUM eurjchem-29 28 2     SPACE eurjchem-29 28 3 nmr nmr NOUN eurjchem-29 28 4     SPACE eurjchem-29 28 5 ( ( PUNCT eurjchem-29 28 6 200 200 NUM eurjchem-29 28 7     SPACE eurjchem-29 28 8 mhz mhz NOUN eurjchem-29 28 9 , , PUNCT eurjchem-29 28 10     SPACE eurjchem-29 28 11 dmso‐d6 dmso‐d6 NOUN eurjchem-29 28 12 ) ) PUNCT eurjchem-29 28 13 , , PUNCT eurjchem-29 28 14     SPACE eurjchem-29 28 15 δ δ PROPN eurjchem-29 28 16 : : PUNCT eurjchem-29 28 17     SPACE eurjchem-29 28 18 1.45 1.45 NUM eurjchem-29 28 19     SPACE eurjchem-29 28 20 ( ( PUNCT eurjchem-29 28 21 t t PROPN eurjchem-29 28 22 , , PUNCT eurjchem-29 28 23     SPACE eurjchem-29 28 24 3h 3h NUM eurjchem-29 28 25 , , PUNCT eurjchem-29 28 26     SPACE eurjchem-29 28 27 ch3 ch3 PROPN eurjchem-29 28 28 ) ) PUNCT eurjchem-29 28 29 , , PUNCT eurjchem-29 28 30     SPACE eurjchem-29 28 31 3.65 3.65 NUM eurjchem-29 28 32     SPACE eurjchem-29 28 33 ( ( PUNCT eurjchem-29 28 34 q q NOUN eurjchem-29 28 35 , , PUNCT eurjchem-29 28 36     SPACE eurjchem-29 28 37 2h 2h NUM eurjchem-29 28 38 , , PUNCT eurjchem-29 28 39     SPACE eurjchem-29 28 40 ch2co ch2co NOUN eurjchem-29 28 41 ) ) PUNCT eurjchem-29 28 42 , , PUNCT eurjchem-29 28 43     SPACE eurjchem-29 28 44 7.64–8.31 7.64–8.31 NUM eurjchem-29 28 45     SPACE eurjchem-29 28 46 ( ( PUNCT eurjchem-29 28 47 m m PROPN eurjchem-29 28 48 , , PUNCT eurjchem-29 28 49     SPACE eurjchem-29 28 50 5h 5h NUM eurjchem-29 28 51 , , PUNCT eurjchem-29 28 52     SPACE eurjchem-29 28 53 ar‐h ar‐h NOUN eurjchem-29 28 54 ) ) PUNCT eurjchem-29 28 55 , , PUNCT eurjchem-29 28 56     SPACE eurjchem-29 28 57 6.39 6.39 NUM eurjchem-29 28 58     SPACE eurjchem-29 28 59 ( ( PUNCT eurjchem-29 28 60 s s PROPN eurjchem-29 28 61 , , PUNCT eurjchem-29 28 62     SPACE eurjchem-29 28 63 1h 1h NUM eurjchem-29 28 64 , , PUNCT eurjchem-29 28 65     SPACE eurjchem-29 28 66 nh nh PROPN eurjchem-29 28 67 ) ) PUNCT eurjchem-29 28 68 . . PUNCT eurjchem-29 28 69     SPACE eurjchem-29 29 1 anal anal ADJ eurjchem-29 29 2 . . PUNCT eurjchem-29 29 3     SPACE eurjchem-29 29 4 calcd calcd NOUN eurjchem-29 29 5 . . PUNCT eurjchem-29 29 6     SPACE eurjchem-29 29 7 for for ADP eurjchem-29 29 8     SPACE eurjchem-29 29 9 c16h11n4o3cl c16h11n4o3cl PROPN eurjchem-29 29 10     SPACE eurjchem-29 29 11 ( ( PUNCT eurjchem-29 29 12 342.5 342.5 NUM eurjchem-29 29 13 ): ): SYM eurjchem-29 29 14     SPACE eurjchem-29 29 15 c c NOUN eurjchem-29 29 16 , , PUNCT eurjchem-29 29 17     SPACE eurjchem-29 29 18 56.05 56.05 NUM eurjchem-29 29 19 ; ; PUNCT eurjchem-29 29 20     SPACE eurjchem-29 29 21 h h NOUN eurjchem-29 29 22 , , PUNCT eurjchem-29 29 23     SPACE eurjchem-29 29 24 3.21 3.21 NUM eurjchem-29 29 25 ; ; PUNCT eurjchem-29 29 26     SPACE eurjchem-29 29 27 n n CCONJ eurjchem-29 29 28 , , PUNCT eurjchem-29 29 29     SPACE eurjchem-29 29 30 16.35 16.35 NUM eurjchem-29 29 31 ; ; PUNCT eurjchem-29 29 32     SPACE eurjchem-29 29 33 cl cl NOUN eurjchem-29 29 34 , , PUNCT eurjchem-29 29 35     SPACE eurjchem-29 29 36 10.36 10.36 NUM eurjchem-29 29 37 . . PUNCT eurjchem-29 29 38     SPACE eurjchem-29 29 39 found find VERB eurjchem-29 29 40 : : PUNCT eurjchem-29 29 41     SPACE eurjchem-29 29 42 c c X eurjchem-29 29 43 , , PUNCT eurjchem-29 29 44     SPACE eurjchem-29 29 45 56.25 56.25 NUM eurjchem-29 29 46 ; ; PUNCT eurjchem-29 29 47     SPACE eurjchem-29 29 48 h h NOUN eurjchem-29 29 49 , , PUNCT eurjchem-29 29 50     SPACE eurjchem-29 29 51 3.52 3.52 NUM eurjchem-29 29 52 ; ; PUNCT eurjchem-29 29 53     SPACE eurjchem-29 29 54 n n CCONJ eurjchem-29 29 55 , , PUNCT eurjchem-29 29 56     SPACE eurjchem-29 29 57 16.67 16.67 NUM eurjchem-29 29 58 ; ; PUNCT eurjchem-29 29 59     SPACE eurjchem-29 29 60 cl cl NOUN eurjchem-29 29 61 , , PUNCT eurjchem-29 29 62     SPACE eurjchem-29 29 63 10.13 10.13 NUM eurjchem-29 29 64 % % NOUN eurjchem-29 29 65 . . PUNCT eurjchem-29 29 66     SPACE eurjchem-29 29 67 compound compound NOUN eurjchem-29 29 68     SPACE eurjchem-29 29 69 3b 3b NOUN eurjchem-29 29 70     SPACE eurjchem-29 29 71 was be AUX eurjchem-29 29 72     SPACE eurjchem-29 29 73 crystallized crystallize VERB eurjchem-29 29 74     SPACE eurjchem-29 29 75 from from ADP eurjchem-29 29 76     SPACE eurjchem-29 29 77 methanol methanol NOUN eurjchem-29 29 78 . . PUNCT eurjchem-29 29 79     SPACE eurjchem-29 29 80 yield yield NOUN eurjchem-29 29 81 : : PUNCT eurjchem-29 29 82     SPACE eurjchem-29 29 83 76 76 NUM eurjchem-29 29 84 % % NOUN eurjchem-29 29 85 . . PUNCT eurjchem-29 29 86     SPACE eurjchem-29 30 1 m.p m.p PROPN eurjchem-29 30 2 . . PROPN eurjchem-29 30 3 : : PUNCT eurjchem-29 30 4     SPACE eurjchem-29 30 5 275‐ 275‐ NUM eurjchem-29 30 6     SPACE eurjchem-29 30 7 278 278 NUM eurjchem-29 30 8     SPACE eurjchem-29 30 9 ºc ºc PROPN eurjchem-29 30 10 . . PUNCT eurjchem-29 30 11     SPACE eurjchem-29 30 12 ft‐ ft‐ PROPN eurjchem-29 30 13     SPACE eurjchem-29 30 14 ir ir PROPN eurjchem-29 30 15     SPACE eurjchem-29 30 16 ( ( PUNCT eurjchem-29 30 17 kbr kbr PROPN eurjchem-29 30 18 ) ) PUNCT eurjchem-29 30 19     SPACE eurjchem-29 30 20 ν ν NOUN eurjchem-29 30 21 , , PUNCT eurjchem-29 30 22     SPACE eurjchem-29 30 23 ( ( PUNCT eurjchem-29 30 24 cm‐1 cm‐1 NOUN eurjchem-29 30 25 ): ): PUNCT eurjchem-29 30 26     SPACE eurjchem-29 30 27 3321 3321 NUM eurjchem-29 30 28     SPACE eurjchem-29 30 29 ( ( PUNCT eurjchem-29 30 30 nh nh NOUN eurjchem-29 30 31 ) ) PUNCT eurjchem-29 30 32 , , PUNCT eurjchem-29 30 33     SPACE eurjchem-29 30 34 2184 2184 NUM eurjchem-29 30 35     SPACE eurjchem-29 30 36 ( ( PUNCT eurjchem-29 30 37 c≡n c≡n PROPN eurjchem-29 30 38 ) ) PUNCT eurjchem-29 30 39 , , PUNCT eurjchem-29 30 40     SPACE eurjchem-29 30 41 1720 1720 NUM eurjchem-29 30 42 , , PUNCT eurjchem-29 30 43     SPACE eurjchem-29 30 44 1680 1680 NUM eurjchem-29 30 45     SPACE eurjchem-29 30 46 ( ( PUNCT eurjchem-29 30 47 2 2 NUM eurjchem-29 30 48     SPACE eurjchem-29 30 49 c c NOUN eurjchem-29 30 50 = = NOUN eurjchem-29 30 51 o o NOUN eurjchem-29 30 52 ) ) PUNCT eurjchem-29 30 53 , , PUNCT eurjchem-29 30 54     SPACE eurjchem-29 30 55 1610 1610 NUM eurjchem-29 30 56     SPACE eurjchem-29 30 57 ( ( PUNCT eurjchem-29 30 58 c c X eurjchem-29 30 59 = = SYM eurjchem-29 30 60 c c NOUN eurjchem-29 30 61 ) ) PUNCT eurjchem-29 30 62 , , PUNCT eurjchem-29 30 63     SPACE eurjchem-29 30 64 1550 1550 NUM eurjchem-29 30 65     SPACE eurjchem-29 30 66 ( ( PUNCT eurjchem-29 30 67 c c NOUN eurjchem-29 30 68 = = SYM eurjchem-29 30 69 n n NUM eurjchem-29 30 70 ) ) PUNCT eurjchem-29 30 71 . . PUNCT eurjchem-29 30 72     SPACE eurjchem-29 31 1 1h 1h NUM eurjchem-29 31 2     SPACE eurjchem-29 31 3 nmr nmr NOUN eurjchem-29 31 4     SPACE eurjchem-29 31 5 ( ( PUNCT eurjchem-29 31 6 200 200 NUM eurjchem-29 31 7     SPACE eurjchem-29 31 8 mhz mhz NOUN eurjchem-29 31 9 , , PUNCT eurjchem-29 31 10     SPACE eurjchem-29 31 11 dmso‐d6 dmso‐d6 NOUN eurjchem-29 31 12 ) ) PUNCT eurjchem-29 31 13 , , PUNCT eurjchem-29 31 14     SPACE eurjchem-29 31 15 δ δ PROPN eurjchem-29 31 16 : : PUNCT eurjchem-29 31 17     SPACE eurjchem-29 31 18 2.52 2.52 NUM eurjchem-29 31 19     SPACE eurjchem-29 31 20 ( ( PUNCT eurjchem-29 31 21 t t PROPN eurjchem-29 31 22 , , PUNCT eurjchem-29 31 23     SPACE eurjchem-29 31 24 3h 3h NUM eurjchem-29 31 25 , , PUNCT eurjchem-29 31 26     SPACE eurjchem-29 31 27 j=8.83hz j=8.83hz PROPN eurjchem-29 31 28 , , PUNCT eurjchem-29 31 29     SPACE eurjchem-29 31 30 ch3 ch3 PROPN eurjchem-29 31 31 ) ) PUNCT eurjchem-29 31 32 , , PUNCT eurjchem-29 31 33     SPACE eurjchem-29 31 34 3.43 3.43 NUM eurjchem-29 31 35     SPACE eurjchem-29 31 36 ( ( PUNCT eurjchem-29 31 37 q q ADJ eurjchem-29 31 38 , , PUNCT eurjchem-29 31 39     SPACE eurjchem-29 31 40 j=32.01 j=32.01 PROPN eurjchem-29 31 41     SPACE eurjchem-29 31 42 hz hz VERB eurjchem-29 31 43 , , PUNCT eurjchem-29 31 44     SPACE eurjchem-29 31 45 2h 2h NUM eurjchem-29 31 46 , , PUNCT eurjchem-29 31 47     SPACE eurjchem-29 31 48 ch2co ch2co NOUN eurjchem-29 31 49 ) ) PUNCT eurjchem-29 31 50 , , PUNCT eurjchem-29 31 51     SPACE eurjchem-29 31 52 7.36–7.70 7.36–7.70 NUM eurjchem-29 31 53     SPACE eurjchem-29 31 54 ( ( PUNCT eurjchem-29 31 55 m m PROPN eurjchem-29 31 56 , , PUNCT eurjchem-29 31 57     SPACE eurjchem-29 31 58 5h 5h NUM eurjchem-29 31 59 , , PUNCT eurjchem-29 31 60     SPACE eurjchem-29 31 61 arh arh ADJ eurjchem-29 31 62 ) ) PUNCT eurjchem-29 31 63 , , PUNCT eurjchem-29 31 64     SPACE eurjchem-29 31 65 6.33 6.33 NUM eurjchem-29 31 66     SPACE eurjchem-29 31 67 ( ( PUNCT eurjchem-29 31 68 s s PROPN eurjchem-29 31 69 , , PUNCT eurjchem-29 31 70     SPACE eurjchem-29 31 71 1h 1h NUM eurjchem-29 31 72 , , PUNCT eurjchem-29 31 73     SPACE eurjchem-29 31 74 nh nh PROPN eurjchem-29 31 75 ) ) PUNCT eurjchem-29 31 76 . . PUNCT eurjchem-29 31 77     SPACE eurjchem-29 32 1 anal.calcd anal.calcd NOUN eurjchem-29 32 2     SPACE eurjchem-29 32 3 for for ADP eurjchem-29 32 4     SPACE eurjchem-29 32 5 c16h11n5o5 c16h11n5o5 NOUN eurjchem-29 32 6     SPACE eurjchem-29 32 7 ( ( PUNCT eurjchem-29 32 8 353 353 NUM eurjchem-29 32 9 ): ): PUNCT eurjchem-29 32 10     SPACE eurjchem-29 32 11 c c NOUN eurjchem-29 32 12 , , PUNCT eurjchem-29 32 13     SPACE eurjchem-29 32 14 54.39 54.39 NUM eurjchem-29 32 15 ; ; PUNCT eurjchem-29 32 16     SPACE eurjchem-29 32 17 h h NOUN eurjchem-29 32 18 , , PUNCT eurjchem-29 32 19     SPACE eurjchem-29 32 20 3.11 3.11 NUM eurjchem-29 32 21 ; ; PUNCT eurjchem-29 32 22     SPACE eurjchem-29 32 23 n n CCONJ eurjchem-29 32 24 , , PUNCT eurjchem-29 32 25     SPACE eurjchem-29 32 26 19.83 19.83 NUM eurjchem-29 32 27 . . PUNCT eurjchem-29 32 28     SPACE eurjchem-29 32 29 found find VERB eurjchem-29 32 30 : : PUNCT eurjchem-29 32 31     SPACE eurjchem-29 32 32 c c X eurjchem-29 32 33 , , PUNCT eurjchem-29 32 34     SPACE eurjchem-29 32 35 54.62 54.62 NUM eurjchem-29 32 36 ; ; PUNCT eurjchem-29 32 37     SPACE eurjchem-29 32 38 h h NOUN eurjchem-29 32 39 , , PUNCT eurjchem-29 32 40     SPACE eurjchem-29 32 41 3.32 3.32 NUM eurjchem-29 32 42 ; ; PUNCT eurjchem-29 32 43     SPACE eurjchem-29 32 44 n n CCONJ eurjchem-29 32 45 , , PUNCT eurjchem-29 32 46     SPACE eurjchem-29 32 47 20.15 20.15 NUM eurjchem-29 32 48 % % NOUN eurjchem-29 32 49 . . PUNCT eurjchem-29 32 50                 SPACE eurjchem-29 32 51 abdel­monem abdel­monem NOUN eurjchem-29 32 52     SPACE eurjchem-29 32 53 / / SYM eurjchem-29 32 54     SPACE eurjchem-29 32 55 european european ADJ eurjchem-29 32 56     SPACE eurjchem-29 32 57 journal journal NOUN eurjchem-29 32 58     SPACE eurjchem-29 32 59 of of ADP eurjchem-29 32 60     SPACE eurjchem-29 32 61 chemistry chemistry NOUN eurjchem-29 32 62     SPACE eurjchem-29 32 63 1 1 NUM eurjchem-29 32 64     SPACE eurjchem-29 32 65 ( ( PUNCT eurjchem-29 32 66 3 3 NUM eurjchem-29 32 67 ) ) PUNCT eurjchem-29 32 68     SPACE eurjchem-29 32 69 ( ( PUNCT eurjchem-29 32 70 2010 2010 NUM eurjchem-29 32 71 ) ) PUNCT eurjchem-29 32 72     SPACE eurjchem-29 32 73 168­172 168­172 NUM eurjchem-29 32 74     SPACE eurjchem-29 32 75 169 169 NUM eurjchem-29 32 76     SPACE eurjchem-29 32 77 scheme scheme NOUN eurjchem-29 32 78     SPACE eurjchem-29 32 79 1 1 NUM eurjchem-29 32 80         SPACE eurjchem-29 32 81 2.2.2 2.2.2 NUM eurjchem-29 32 82 . . PUNCT eurjchem-29 32 83     SPACE eurjchem-29 33 1 7­(4­chloro/3­nitrophenyl)­6­cyano­5­oxo­1,5­ 7­(4­chloro/3­nitrophenyl)­6­cyano­5­oxo­1,5­ NUM eurjchem-29 33 2 dihydro[1,2,4]triazolo[1,5­a]pyridine­8­carbohydrazide dihydro[1,2,4]triazolo[1,5­a]pyridine­8­carbohydrazide ADV eurjchem-29 33 3     SPACE eurjchem-29 33 4 ( ( PUNCT eurjchem-29 33 5 4a 4a NUM eurjchem-29 33 6 , , PUNCT eurjchem-29 33 7 b b NOUN eurjchem-29 33 8 ) ) PUNCT eurjchem-29 33 9         SPACE eurjchem-29 33 10 a a DET eurjchem-29 33 11     SPACE eurjchem-29 33 12 mixture mixture NOUN eurjchem-29 33 13     SPACE eurjchem-29 33 14 of of ADP eurjchem-29 33 15     SPACE eurjchem-29 33 16 compounds compound NOUN eurjchem-29 33 17     SPACE eurjchem-29 33 18 3a 3a NUM eurjchem-29 33 19 , , PUNCT eurjchem-29 33 20     SPACE eurjchem-29 33 21 b b NOUN eurjchem-29 33 22     SPACE eurjchem-29 33 23 ( ( PUNCT eurjchem-29 33 24 0.01 0.01 NUM eurjchem-29 33 25     SPACE eurjchem-29 33 26 mol mol NOUN eurjchem-29 33 27 ) ) PUNCT eurjchem-29 33 28     SPACE eurjchem-29 33 29 and and CCONJ eurjchem-29 33 30     SPACE eurjchem-29 33 31 hydrazine hydrazine NOUN eurjchem-29 33 32     SPACE eurjchem-29 33 33 hydrate hydrate NOUN eurjchem-29 33 34     SPACE eurjchem-29 33 35 98 98 NUM eurjchem-29 33 36 % % NOUN eurjchem-29 33 37     SPACE eurjchem-29 33 38 ( ( PUNCT eurjchem-29 33 39 0.015 0.015 NUM eurjchem-29 33 40     SPACE eurjchem-29 33 41 mol mol NOUN eurjchem-29 33 42 ) ) PUNCT eurjchem-29 33 43     SPACE eurjchem-29 33 44 in in ADP eurjchem-29 33 45     SPACE eurjchem-29 33 46 tetrahydrofuran tetrahydrofuran NOUN eurjchem-29 33 47     SPACE eurjchem-29 33 48 ( ( PUNCT eurjchem-29 33 49 20 20 NUM eurjchem-29 33 50     SPACE eurjchem-29 33 51 cm3 cm3 NOUN eurjchem-29 33 52 ) ) PUNCT eurjchem-29 33 53     SPACE eurjchem-29 33 54 was be AUX eurjchem-29 33 55     SPACE eurjchem-29 33 56 heated heated ADJ eurjchem-29 33 57     SPACE eurjchem-29 33 58 under under ADP eurjchem-29 33 59     SPACE eurjchem-29 33 60 reflux reflux NOUN eurjchem-29 33 61     SPACE eurjchem-29 33 62 for for ADP eurjchem-29 33 63     SPACE eurjchem-29 33 64 5 5 NUM eurjchem-29 33 65     SPACE eurjchem-29 33 66 h h NOUN eurjchem-29 33 67     SPACE eurjchem-29 33 68 and and CCONJ eurjchem-29 33 69     SPACE eurjchem-29 33 70 then then ADV eurjchem-29 33 71     SPACE eurjchem-29 33 72 allowed allow VERB eurjchem-29 33 73     SPACE eurjchem-29 33 74 to to PART eurjchem-29 33 75     SPACE eurjchem-29 33 76 cool cool ADJ eurjchem-29 33 77 . . PUNCT eurjchem-29 33 78     SPACE eurjchem-29 34 1 the the DET eurjchem-29 34 2     SPACE eurjchem-29 34 3 precipitate precipitate NOUN eurjchem-29 34 4     SPACE eurjchem-29 34 5 that that PRON eurjchem-29 34 6     SPACE eurjchem-29 34 7 formed form VERB eurjchem-29 34 8     SPACE eurjchem-29 34 9 was be AUX eurjchem-29 34 10     SPACE eurjchem-29 34 11 filtered filter VERB eurjchem-29 34 12     SPACE eurjchem-29 34 13 off off ADP eurjchem-29 34 14 , , PUNCT eurjchem-29 34 15     SPACE eurjchem-29 34 16 dried dry VERB eurjchem-29 34 17     SPACE eurjchem-29 34 18 and and CCONJ eurjchem-29 34 19     SPACE eurjchem-29 34 20 crystallized crystallize VERB eurjchem-29 34 21     SPACE eurjchem-29 34 22 to to PART eurjchem-29 34 23     SPACE eurjchem-29 34 24 give give VERB eurjchem-29 34 25     SPACE eurjchem-29 34 26 compounds compound NOUN eurjchem-29 34 27     SPACE eurjchem-29 34 28 4a 4a NOUN eurjchem-29 34 29 , , PUNCT eurjchem-29 34 30     SPACE eurjchem-29 34 31 b b NOUN eurjchem-29 34 32 , , PUNCT eurjchem-29 34 33     SPACE eurjchem-29 34 34 respectively respectively ADV eurjchem-29 34 35     SPACE eurjchem-29 34 36 ( ( PUNCT eurjchem-29 34 37 scheme scheme NOUN eurjchem-29 34 38     SPACE eurjchem-29 34 39 1 1 NUM eurjchem-29 34 40 ) ) PUNCT eurjchem-29 34 41 . . PUNCT eurjchem-29 34 42     SPACE eurjchem-29 34 43 compound compound NOUN eurjchem-29 34 44     SPACE eurjchem-29 34 45 4a 4a NOUN eurjchem-29 34 46     SPACE eurjchem-29 34 47 was be AUX eurjchem-29 34 48     SPACE eurjchem-29 34 49 crystallized crystallize VERB eurjchem-29 34 50     SPACE eurjchem-29 34 51 from from ADP eurjchem-29 34 52     SPACE eurjchem-29 34 53 a a DET eurjchem-29 34 54     SPACE eurjchem-29 34 55 mixture mixture NOUN eurjchem-29 34 56     SPACE eurjchem-29 34 57 of of ADP eurjchem-29 34 58     SPACE eurjchem-29 34 59 methanol methanol NOUN eurjchem-29 34 60     SPACE eurjchem-29 34 61 and and CCONJ eurjchem-29 34 62     SPACE eurjchem-29 34 63 dmf dmf PROPN eurjchem-29 34 64     SPACE eurjchem-29 34 65 ( ( PUNCT eurjchem-29 34 66 1:1).yield 1:1).yield NUM eurjchem-29 34 67 : : PUNCT eurjchem-29 34 68     SPACE eurjchem-29 34 69 65 65 NUM eurjchem-29 34 70 % % NOUN eurjchem-29 34 71 . . PUNCT eurjchem-29 34 72     SPACE eurjchem-29 35 1 m.p m.p PROPN eurjchem-29 35 2 . . PROPN eurjchem-29 35 3 : : PUNCT eurjchem-29 35 4     SPACE eurjchem-29 35 5 187‐189 187‐189 NUM eurjchem-29 35 6     SPACE eurjchem-29 35 7 ºc ºc PROPN eurjchem-29 35 8 . . PUNCT eurjchem-29 35 9     SPACE eurjchem-29 35 10 ft‐ ft‐ PROPN eurjchem-29 35 11     SPACE eurjchem-29 35 12 ir ir PROPN eurjchem-29 35 13     SPACE eurjchem-29 35 14 ( ( PUNCT eurjchem-29 35 15 kbr kbr PROPN eurjchem-29 35 16 ) ) PUNCT eurjchem-29 35 17     SPACE eurjchem-29 35 18 ν ν PROPN eurjchem-29 35 19 , , PUNCT eurjchem-29 35 20       SPACE eurjchem-29 35 21 ( ( PUNCT eurjchem-29 35 22 cm‐1 cm‐1 NOUN eurjchem-29 35 23 ): ): PUNCT eurjchem-29 35 24         SPACE eurjchem-29 35 25 3412 3412 NUM eurjchem-29 35 26 , , PUNCT eurjchem-29 35 27     SPACE eurjchem-29 35 28 3341 3341 NUM eurjchem-29 35 29 , , PUNCT eurjchem-29 35 30     SPACE eurjchem-29 35 31 3262 3262 NUM eurjchem-29 35 32 , , PUNCT eurjchem-29 35 33     SPACE eurjchem-29 35 34 31800 31800 NUM eurjchem-29 35 35     SPACE eurjchem-29 35 36 ( ( PUNCT eurjchem-29 35 37 nh2 nh2 PROPN eurjchem-29 35 38 , , PUNCT eurjchem-29 35 39     SPACE eurjchem-29 35 40 2nh 2nh NOUN eurjchem-29 35 41 ) ) PUNCT eurjchem-29 35 42 , , PUNCT eurjchem-29 35 43     SPACE eurjchem-29 35 44 2213 2213 NUM eurjchem-29 35 45     SPACE eurjchem-29 35 46 ( ( PUNCT eurjchem-29 35 47 c≡n c≡n PROPN eurjchem-29 35 48 ) ) PUNCT eurjchem-29 35 49 , , PUNCT eurjchem-29 35 50     SPACE eurjchem-29 35 51 1736 1736 NUM eurjchem-29 35 52 , , PUNCT eurjchem-29 35 53     SPACE eurjchem-29 35 54 1676 1676 NUM eurjchem-29 35 55     SPACE eurjchem-29 35 56 ( ( PUNCT eurjchem-29 35 57 2c 2c NOUN eurjchem-29 35 58 = = SYM eurjchem-29 35 59 o o NOUN eurjchem-29 35 60 ) ) PUNCT eurjchem-29 35 61 , , PUNCT eurjchem-29 35 62     SPACE eurjchem-29 35 63 1626 1626 NUM eurjchem-29 35 64     SPACE eurjchem-29 35 65 ( ( PUNCT eurjchem-29 35 66 c c X eurjchem-29 35 67 = = SYM eurjchem-29 35 68 c c NOUN eurjchem-29 35 69 ) ) PUNCT eurjchem-29 35 70 , , PUNCT eurjchem-29 35 71     SPACE eurjchem-29 35 72 1576 1576 NUM eurjchem-29 35 73     SPACE eurjchem-29 35 74 ( ( PUNCT eurjchem-29 35 75 c c NOUN eurjchem-29 35 76 = = SYM eurjchem-29 35 77 n n NUM eurjchem-29 35 78 ) ) PUNCT eurjchem-29 35 79 , , PUNCT eurjchem-29 35 80     SPACE eurjchem-29 35 81 721 721 NUM eurjchem-29 35 82     SPACE eurjchem-29 35 83 ( ( PUNCT eurjchem-29 35 84 c‐cl c‐cl PROPN eurjchem-29 35 85 ) ) PUNCT eurjchem-29 35 86 . . PUNCT eurjchem-29 35 87     SPACE eurjchem-29 35 88 1h 1h NUM eurjchem-29 35 89     SPACE eurjchem-29 35 90 nmr nmr NOUN eurjchem-29 35 91     SPACE eurjchem-29 35 92 ( ( PUNCT eurjchem-29 35 93 200 200 NUM eurjchem-29 35 94     SPACE eurjchem-29 35 95 mhz mhz NOUN eurjchem-29 35 96 , , PUNCT eurjchem-29 35 97     SPACE eurjchem-29 35 98 dmso‐d6 dmso‐d6 NOUN eurjchem-29 35 99 ) ) PUNCT eurjchem-29 35 100 , , PUNCT eurjchem-29 35 101     SPACE eurjchem-29 35 102 δ δ PROPN eurjchem-29 35 103 : : PUNCT eurjchem-29 35 104     SPACE eurjchem-29 35 105 4.36 4.36 NUM eurjchem-29 35 106     SPACE eurjchem-29 35 107 ( ( PUNCT eurjchem-29 35 108 s s PROPN eurjchem-29 35 109 , , PUNCT eurjchem-29 35 110     SPACE eurjchem-29 35 111 br br PROPN eurjchem-29 35 112 , , PUNCT eurjchem-29 35 113     SPACE eurjchem-29 35 114 2h 2h NUM eurjchem-29 35 115 , , PUNCT eurjchem-29 35 116     SPACE eurjchem-29 35 117 nh2 nh2 PROPN eurjchem-29 35 118 ) ) PUNCT eurjchem-29 35 119 , , PUNCT eurjchem-29 35 120     SPACE eurjchem-29 35 121 7.28–7.91 7.28–7.91 NUM eurjchem-29 35 122     SPACE eurjchem-29 35 123 ( ( PUNCT eurjchem-29 35 124 m m PROPN eurjchem-29 35 125 , , PUNCT eurjchem-29 35 126     SPACE eurjchem-29 35 127 5h 5h NUM eurjchem-29 35 128 , , PUNCT eurjchem-29 35 129     SPACE eurjchem-29 35 130 arh arh ADJ eurjchem-29 35 131 ) ) PUNCT eurjchem-29 35 132 , , PUNCT eurjchem-29 35 133     SPACE eurjchem-29 35 134 5.75 5.75 NUM eurjchem-29 35 135     SPACE eurjchem-29 35 136 and and CCONJ eurjchem-29 35 137     SPACE eurjchem-29 35 138 8.75 8.75 NUM eurjchem-29 35 139     SPACE eurjchem-29 35 140 ( ( PUNCT eurjchem-29 35 141 2s 2s NUM eurjchem-29 35 142 , , PUNCT eurjchem-29 35 143     SPACE eurjchem-29 35 144 2h 2h NUM eurjchem-29 35 145 , , PUNCT eurjchem-29 35 146     SPACE eurjchem-29 35 147 2nh 2nh NOUN eurjchem-29 35 148 ) ) PUNCT eurjchem-29 35 149 . . PUNCT eurjchem-29 35 150     SPACE eurjchem-29 36 1 anal anal ADJ eurjchem-29 36 2 . . PUNCT eurjchem-29 36 3     SPACE eurjchem-29 36 4 calcd calcd NOUN eurjchem-29 36 5 . . PUNCT eurjchem-29 36 6     SPACE eurjchem-29 36 7 for for ADP eurjchem-29 36 8     SPACE eurjchem-29 36 9 c14h9n6o2cl c14h9n6o2cl NOUN eurjchem-29 36 10     SPACE eurjchem-29 36 11 ( ( PUNCT eurjchem-29 36 12 328.5 328.5 NUM eurjchem-29 36 13 ): ): SYM eurjchem-29 36 14     SPACE eurjchem-29 36 15 c c NOUN eurjchem-29 36 16 , , PUNCT eurjchem-29 36 17     SPACE eurjchem-29 36 18 51.14 51.14 NUM eurjchem-29 36 19 ; ; PUNCT eurjchem-29 36 20     SPACE eurjchem-29 36 21 h h NOUN eurjchem-29 36 22 , , PUNCT eurjchem-29 36 23     SPACE eurjchem-29 36 24 2.73 2.73 NUM eurjchem-29 36 25 ; ; PUNCT eurjchem-29 36 26     SPACE eurjchem-29 36 27 n n CCONJ eurjchem-29 36 28 , , PUNCT eurjchem-29 36 29     SPACE eurjchem-29 36 30 25.57 25.57 NUM eurjchem-29 36 31 ; ; PUNCT eurjchem-29 36 32     SPACE eurjchem-29 36 33 cl cl NOUN eurjchem-29 36 34 , , PUNCT eurjchem-29 36 35     SPACE eurjchem-29 36 36 10.80 10.80 NUM eurjchem-29 36 37 . . PUNCT eurjchem-29 36 38     SPACE eurjchem-29 36 39 found find VERB eurjchem-29 36 40 : : PUNCT eurjchem-29 36 41     SPACE eurjchem-29 36 42 c c X eurjchem-29 36 43 , , PUNCT eurjchem-29 36 44     SPACE eurjchem-29 36 45 51.43 51.43 NUM eurjchem-29 36 46 ; ; PUNCT eurjchem-29 36 47     SPACE eurjchem-29 36 48 h h NOUN eurjchem-29 36 49 , , PUNCT eurjchem-29 36 50     SPACE eurjchem-29 36 51 3.01 3.01 NUM eurjchem-29 36 52 ; ; PUNCT eurjchem-29 36 53     SPACE eurjchem-29 36 54 n n CCONJ eurjchem-29 36 55 , , PUNCT eurjchem-29 36 56     SPACE eurjchem-29 36 57 25.93 25.93 NUM eurjchem-29 36 58 ; ; PUNCT eurjchem-29 36 59     SPACE eurjchem-29 36 60 cl cl NOUN eurjchem-29 36 61 , , PUNCT eurjchem-29 36 62     SPACE eurjchem-29 36 63 10.45 10.45 NUM eurjchem-29 36 64 % % NOUN eurjchem-29 36 65 . . PUNCT eurjchem-29 36 66       SPACE eurjchem-29 37 1 compound compound PROPN eurjchem-29 37 2     SPACE eurjchem-29 37 3 4b 4b PROPN eurjchem-29 37 4     SPACE eurjchem-29 37 5 was be AUX eurjchem-29 37 6     SPACE eurjchem-29 37 7 crystallized crystallize VERB eurjchem-29 37 8     SPACE eurjchem-29 37 9 from from ADP eurjchem-29 37 10     SPACE eurjchem-29 37 11 ethanol ethanol NOUN eurjchem-29 37 12 . . PUNCT eurjchem-29 37 13     SPACE eurjchem-29 37 14 yield yield NOUN eurjchem-29 37 15 : : PUNCT eurjchem-29 37 16     SPACE eurjchem-29 37 17 67 67 NUM eurjchem-29 37 18     SPACE eurjchem-29 37 19 % % NOUN eurjchem-29 37 20 . . PUNCT eurjchem-29 37 21     SPACE eurjchem-29 38 1 m.p m.p PROPN eurjchem-29 38 2 . . PROPN eurjchem-29 38 3 : : PUNCT eurjchem-29 38 4     SPACE eurjchem-29 38 5 177‐179 177‐179 PROPN eurjchem-29 38 6     SPACE eurjchem-29 38 7 ºc ºc PROPN eurjchem-29 38 8 . . PUNCT eurjchem-29 38 9         SPACE eurjchem-29 38 10 ft‐ ft‐ PROPN eurjchem-29 38 11     SPACE eurjchem-29 38 12 ir ir PROPN eurjchem-29 38 13     SPACE eurjchem-29 38 14 ( ( PUNCT eurjchem-29 38 15 kbr kbr PROPN eurjchem-29 38 16 ) ) PUNCT eurjchem-29 38 17     SPACE eurjchem-29 38 18 ν ν NOUN eurjchem-29 38 19 , , PUNCT eurjchem-29 38 20     SPACE eurjchem-29 38 21 ( ( PUNCT eurjchem-29 38 22 cm‐1 cm‐1 NOUN eurjchem-29 38 23 ): ): PUNCT eurjchem-29 38 24     SPACE eurjchem-29 38 25 3423 3423 NUM eurjchem-29 38 26 , , PUNCT eurjchem-29 38 27     SPACE eurjchem-29 38 28 3356 3356 NUM eurjchem-29 38 29 , , PUNCT eurjchem-29 38 30     SPACE eurjchem-29 38 31 3272 3272 NUM eurjchem-29 38 32 , , PUNCT eurjchem-29 38 33     SPACE eurjchem-29 38 34 2289 2289 NUM eurjchem-29 38 35     SPACE eurjchem-29 38 36 ( ( PUNCT eurjchem-29 38 37 nh2 nh2 PROPN eurjchem-29 38 38 , , PUNCT eurjchem-29 38 39     SPACE eurjchem-29 38 40 2nh 2nh NOUN eurjchem-29 38 41 ) ) PUNCT eurjchem-29 38 42 , , PUNCT eurjchem-29 38 43     SPACE eurjchem-29 38 44 1729 1729 NUM eurjchem-29 38 45 , , PUNCT eurjchem-29 38 46     SPACE eurjchem-29 38 47 1696 1696 NUM eurjchem-29 38 48     SPACE eurjchem-29 38 49 ( ( PUNCT eurjchem-29 38 50 2c 2c NOUN eurjchem-29 38 51 = = SYM eurjchem-29 38 52 o o NOUN eurjchem-29 38 53 ) ) PUNCT eurjchem-29 38 54 , , PUNCT eurjchem-29 38 55     SPACE eurjchem-29 38 56 1624 1624 NUM eurjchem-29 38 57     SPACE eurjchem-29 38 58 ( ( PUNCT eurjchem-29 38 59 c c X eurjchem-29 38 60 = = SYM eurjchem-29 38 61 c c NOUN eurjchem-29 38 62 ) ) PUNCT eurjchem-29 38 63 , , PUNCT eurjchem-29 38 64     SPACE eurjchem-29 38 65 2218 2218 NUM eurjchem-29 38 66     SPACE eurjchem-29 38 67 ( ( PUNCT eurjchem-29 38 68 c≡n c≡n PROPN eurjchem-29 38 69 ) ) PUNCT eurjchem-29 38 70 , , PUNCT eurjchem-29 38 71     SPACE eurjchem-29 38 72 1556 1556 NUM eurjchem-29 38 73     SPACE eurjchem-29 38 74 ( ( PUNCT eurjchem-29 38 75 c c NOUN eurjchem-29 38 76 = = SYM eurjchem-29 38 77 n n NUM eurjchem-29 38 78 ) ) PUNCT eurjchem-29 38 79 . . PUNCT eurjchem-29 38 80     SPACE eurjchem-29 38 81 1h 1h NUM eurjchem-29 38 82     SPACE eurjchem-29 38 83 nmr nmr NOUN eurjchem-29 38 84     SPACE eurjchem-29 38 85 ( ( PUNCT eurjchem-29 38 86 200 200 NUM eurjchem-29 38 87     SPACE eurjchem-29 38 88 mhz mhz NOUN eurjchem-29 38 89 , , PUNCT eurjchem-29 38 90     SPACE eurjchem-29 38 91 dmso‐d6 dmso‐d6 NOUN eurjchem-29 38 92 ) ) PUNCT eurjchem-29 38 93 , , PUNCT eurjchem-29 38 94     SPACE eurjchem-29 38 95 δ δ PROPN eurjchem-29 38 96 : : PUNCT eurjchem-29 38 97     SPACE eurjchem-29 38 98 5.42 5.42 NUM eurjchem-29 38 99     SPACE eurjchem-29 38 100 ( ( PUNCT eurjchem-29 38 101 s s PROPN eurjchem-29 38 102 , , PUNCT eurjchem-29 38 103     SPACE eurjchem-29 38 104 br br PROPN eurjchem-29 38 105 , , PUNCT eurjchem-29 38 106     SPACE eurjchem-29 38 107 2h 2h NUM eurjchem-29 38 108 , , PUNCT eurjchem-29 38 109     SPACE eurjchem-29 38 110 nh2 nh2 PROPN eurjchem-29 38 111 ) ) PUNCT eurjchem-29 38 112 , , PUNCT eurjchem-29 38 113     SPACE eurjchem-29 38 114 6.95–7.76 6.95–7.76 NUM eurjchem-29 38 115     SPACE eurjchem-29 38 116 ( ( PUNCT eurjchem-29 38 117 m m PROPN eurjchem-29 38 118 , , PUNCT eurjchem-29 38 119     SPACE eurjchem-29 38 120 5h 5h NUM eurjchem-29 38 121 , , PUNCT eurjchem-29 38 122     SPACE eurjchem-29 38 123 ar‐h ar‐h NOUN eurjchem-29 38 124 ) ) PUNCT eurjchem-29 38 125 , , PUNCT eurjchem-29 38 126     SPACE eurjchem-29 38 127 6.76 6.76 NUM eurjchem-29 38 128     SPACE eurjchem-29 38 129 ( ( PUNCT eurjchem-29 38 130 s s PROPN eurjchem-29 38 131 , , PUNCT eurjchem-29 38 132     SPACE eurjchem-29 38 133 1h 1h NUM eurjchem-29 38 134 , , PUNCT eurjchem-29 38 135     SPACE eurjchem-29 38 136 1nh 1nh NOUN eurjchem-29 38 137 ) ) PUNCT eurjchem-29 38 138 , , PUNCT eurjchem-29 38 139     SPACE eurjchem-29 38 140 8.85 8.85 NUM eurjchem-29 38 141     SPACE eurjchem-29 38 142 ( ( PUNCT eurjchem-29 38 143 s s PROPN eurjchem-29 38 144 , , PUNCT eurjchem-29 38 145     SPACE eurjchem-29 38 146 1h 1h NUM eurjchem-29 38 147 , , PUNCT eurjchem-29 38 148     SPACE eurjchem-29 38 149 1nh 1nh NOUN eurjchem-29 38 150 ) ) PUNCT eurjchem-29 38 151 . . PUNCT eurjchem-29 38 152     SPACE eurjchem-29 39 1 anal anal ADJ eurjchem-29 39 2 . . PUNCT eurjchem-29 39 3     SPACE eurjchem-29 39 4 calcd calcd NOUN eurjchem-29 39 5 . . PUNCT eurjchem-29 39 6     SPACE eurjchem-29 39 7 for for ADP eurjchem-29 39 8     SPACE eurjchem-29 39 9 c14h9n7o4 c14h9n7o4 PROPN eurjchem-29 39 10     SPACE eurjchem-29 39 11 ( ( PUNCT eurjchem-29 39 12 339 339 NUM eurjchem-29 39 13 ): ): PUNCT eurjchem-29 39 14     SPACE eurjchem-29 39 15 c c NOUN eurjchem-29 39 16 , , PUNCT eurjchem-29 39 17     SPACE eurjchem-29 39 18 49.55 49.55 NUM eurjchem-29 39 19 ; ; PUNCT eurjchem-29 39 20     SPACE eurjchem-29 39 21 h h NOUN eurjchem-29 39 22 , , PUNCT eurjchem-29 39 23     SPACE eurjchem-29 39 24 2.65 2.65 NUM eurjchem-29 39 25 ; ; PUNCT eurjchem-29 39 26     SPACE eurjchem-29 39 27 n n CCONJ eurjchem-29 39 28 , , PUNCT eurjchem-29 39 29     SPACE eurjchem-29 39 30 28.90 28.90 NUM eurjchem-29 39 31 . . PUNCT eurjchem-29 39 32     SPACE eurjchem-29 39 33 found find VERB eurjchem-29 39 34 : : PUNCT eurjchem-29 39 35     SPACE eurjchem-29 39 36 c c X eurjchem-29 39 37 , , PUNCT eurjchem-29 39 38     SPACE eurjchem-29 39 39 50.03 50.03 NUM eurjchem-29 39 40 ; ; PUNCT eurjchem-29 39 41     SPACE eurjchem-29 39 42 h h NOUN eurjchem-29 39 43 , , PUNCT eurjchem-29 39 44     SPACE eurjchem-29 39 45 2.94 2.94 NUM eurjchem-29 39 46 ; ; PUNCT eurjchem-29 39 47     SPACE eurjchem-29 39 48 n n CCONJ eurjchem-29 39 49 , , PUNCT eurjchem-29 39 50     SPACE eurjchem-29 39 51 28.55 28.55 NUM eurjchem-29 39 52 % % NOUN eurjchem-29 39 53 . . PUNCT eurjchem-29 39 54           SPACE eurjchem-29 40 1 2.2.3 2.2.3 NUM eurjchem-29 40 2 . . PUNCT eurjchem-29 40 3     SPACE eurjchem-29 41 1 7­(4­chloro/3­nitrophenyl)­8­(5,6­diphenyl­4h­1,3,4­ 7­(4­chloro/3­nitrophenyl)­8­(5,6­diphenyl­4h­1,3,4­ NUM eurjchem-29 41 2 oxadiazin­2­yl)­5­oxo­1,5­dihydro[1,2,4]triazolo[1,5­ oxadiazin­2­yl)­5­oxo­1,5­dihydro[1,2,4]triazolo[1,5­ NUM eurjchem-29 41 3 a]pyridine­6­carbonitrile a]pyridine­6­carbonitrile ADJ eurjchem-29 41 4     SPACE eurjchem-29 41 5 ( ( PUNCT eurjchem-29 41 6 5a 5a NUM eurjchem-29 41 7 , , PUNCT eurjchem-29 41 8 b b NOUN eurjchem-29 41 9 ) ) PUNCT eurjchem-29 41 10         SPACE eurjchem-29 41 11 a a DET eurjchem-29 41 12     SPACE eurjchem-29 41 13 mixture mixture NOUN eurjchem-29 41 14     SPACE eurjchem-29 41 15 of of ADP eurjchem-29 41 16     SPACE eurjchem-29 41 17 compounds compound NOUN eurjchem-29 41 18     SPACE eurjchem-29 41 19 4a 4a NOUN eurjchem-29 41 20 , , PUNCT eurjchem-29 41 21     SPACE eurjchem-29 41 22 b b NOUN eurjchem-29 41 23     SPACE eurjchem-29 41 24 ( ( PUNCT eurjchem-29 41 25 0.01 0.01 NUM eurjchem-29 41 26     SPACE eurjchem-29 41 27 mol mol NOUN eurjchem-29 41 28 ) ) PUNCT eurjchem-29 41 29     SPACE eurjchem-29 41 30 and and CCONJ eurjchem-29 41 31     SPACE eurjchem-29 41 32 2‐hydroxy‐ 2‐hydroxy‐ NUM eurjchem-29 41 33 1,2‐diphenylethanone 1,2‐diphenylethanone NUM eurjchem-29 41 34     SPACE eurjchem-29 41 35 ( ( PUNCT eurjchem-29 41 36 0.01 0.01 NUM eurjchem-29 41 37     SPACE eurjchem-29 41 38 mol mol NOUN eurjchem-29 41 39 ) ) PUNCT eurjchem-29 41 40     SPACE eurjchem-29 41 41 in in ADP eurjchem-29 41 42     SPACE eurjchem-29 41 43 dmf dmf PROPN eurjchem-29 41 44     SPACE eurjchem-29 41 45 ( ( PUNCT eurjchem-29 41 46 20 20 NUM eurjchem-29 41 47     SPACE eurjchem-29 41 48 cm3 cm3 NOUN eurjchem-29 41 49 ) ) PUNCT eurjchem-29 41 50     SPACE eurjchem-29 41 51 was be AUX eurjchem-29 41 52     SPACE eurjchem-29 41 53 refluxed refluxe VERB eurjchem-29 41 54     SPACE eurjchem-29 41 55 for for ADP eurjchem-29 41 56     SPACE eurjchem-29 41 57 8 8 NUM eurjchem-29 41 58     SPACE eurjchem-29 41 59 h h NOUN eurjchem-29 41 60 , , PUNCT eurjchem-29 41 61     SPACE eurjchem-29 41 62 and and CCONJ eurjchem-29 41 63     SPACE eurjchem-29 41 64 then then ADV eurjchem-29 41 65     SPACE eurjchem-29 41 66 allowed allow VERB eurjchem-29 41 67     SPACE eurjchem-29 41 68 to to PART eurjchem-29 41 69     SPACE eurjchem-29 41 70 cool cool ADJ eurjchem-29 41 71 . . PUNCT eurjchem-29 41 72     SPACE eurjchem-29 42 1 the the DET eurjchem-29 42 2     SPACE eurjchem-29 42 3 reaction reaction NOUN eurjchem-29 42 4     SPACE eurjchem-29 42 5 mixture mixture NOUN eurjchem-29 42 6     SPACE eurjchem-29 42 7 was be AUX eurjchem-29 42 8     SPACE eurjchem-29 42 9 poured pour VERB eurjchem-29 42 10     SPACE eurjchem-29 42 11 onto onto ADP eurjchem-29 42 12     SPACE eurjchem-29 42 13 ice‐water ice‐water NOUN eurjchem-29 42 14 . . PUNCT eurjchem-29 42 15     SPACE eurjchem-29 43 1 the the DET eurjchem-29 43 2     SPACE eurjchem-29 43 3 solid solid ADJ eurjchem-29 43 4     SPACE eurjchem-29 43 5 product product NOUN eurjchem-29 43 6     SPACE eurjchem-29 43 7 that that PRON eurjchem-29 43 8     SPACE eurjchem-29 43 9 formed form VERB eurjchem-29 43 10     SPACE eurjchem-29 43 11 was be AUX eurjchem-29 43 12     SPACE eurjchem-29 43 13 filtered filter VERB eurjchem-29 43 14     SPACE eurjchem-29 43 15 off off ADP eurjchem-29 43 16 , , PUNCT eurjchem-29 43 17     SPACE eurjchem-29 43 18 dried dry VERB eurjchem-29 43 19     SPACE eurjchem-29 43 20 and and CCONJ eurjchem-29 43 21     SPACE eurjchem-29 43 22 crystallized crystallize VERB eurjchem-29 43 23     SPACE eurjchem-29 43 24 to to PART eurjchem-29 43 25     SPACE eurjchem-29 43 26 give give VERB eurjchem-29 43 27     SPACE eurjchem-29 43 28 compounds compound NOUN eurjchem-29 43 29     SPACE eurjchem-29 43 30 5a 5a NUM eurjchem-29 43 31 , , PUNCT eurjchem-29 43 32     SPACE eurjchem-29 43 33 b b NOUN eurjchem-29 43 34 , , PUNCT eurjchem-29 43 35     SPACE eurjchem-29 43 36 respectively respectively ADV eurjchem-29 43 37     SPACE eurjchem-29 43 38 ( ( PUNCT eurjchem-29 43 39 scheme scheme NOUN eurjchem-29 43 40     SPACE eurjchem-29 43 41 1 1 NUM eurjchem-29 43 42 ) ) PUNCT eurjchem-29 43 43 . . PUNCT eurjchem-29 43 44     SPACE eurjchem-29 44 1 compound compound VERB eurjchem-29 44 2     SPACE eurjchem-29 44 3 5a 5a NUM eurjchem-29 44 4     SPACE eurjchem-29 44 5 was be AUX eurjchem-29 44 6     SPACE eurjchem-29 44 7 crystallized crystallize VERB eurjchem-29 44 8     SPACE eurjchem-29 44 9 from from ADP eurjchem-29 44 10     SPACE eurjchem-29 44 11 isopropanol isopropanol NOUN eurjchem-29 44 12 . . PUNCT eurjchem-29 44 13     SPACE eurjchem-29 44 14 yield yield NOUN eurjchem-29 44 15 : : PUNCT eurjchem-29 44 16     SPACE eurjchem-29 44 17 62 62 NUM eurjchem-29 44 18     SPACE eurjchem-29 44 19 % % NOUN eurjchem-29 44 20 . . PUNCT eurjchem-29 44 21     SPACE eurjchem-29 45 1 m.p m.p PROPN eurjchem-29 45 2 . . PROPN eurjchem-29 45 3 : : PUNCT eurjchem-29 45 4     SPACE eurjchem-29 45 5 210–212 210–212 NUM eurjchem-29 45 6     SPACE eurjchem-29 45 7 ºc ºc PROPN eurjchem-29 45 8 . . PUNCT eurjchem-29 45 9       SPACE eurjchem-29 45 10 ft‐ir ft‐ir NOUN eurjchem-29 45 11     SPACE eurjchem-29 45 12 ( ( PUNCT eurjchem-29 45 13 kbr kbr PROPN eurjchem-29 45 14 ) ) PUNCT eurjchem-29 45 15     SPACE eurjchem-29 45 16 ν ν PROPN eurjchem-29 45 17 , , PUNCT eurjchem-29 45 18     SPACE eurjchem-29 45 19 ( ( PUNCT eurjchem-29 45 20 cm‐1 cm‐1 NOUN eurjchem-29 45 21 ): ): PUNCT eurjchem-29 45 22     SPACE eurjchem-29 45 23 3344 3344 NUM eurjchem-29 45 24 , , PUNCT eurjchem-29 45 25     SPACE eurjchem-29 45 26 3206 3206 NUM eurjchem-29 45 27     SPACE eurjchem-29 45 28 ( ( PUNCT eurjchem-29 45 29 2nh 2nh PROPN eurjchem-29 45 30 ) ) PUNCT eurjchem-29 45 31 , , PUNCT eurjchem-29 45 32     SPACE eurjchem-29 45 33 1784 1784 NUM eurjchem-29 45 34     SPACE eurjchem-29 45 35 ( ( PUNCT eurjchem-29 45 36 c c NOUN eurjchem-29 45 37 = = NOUN eurjchem-29 45 38 o o NOUN eurjchem-29 45 39 ) ) PUNCT eurjchem-29 45 40 , , PUNCT eurjchem-29 45 41     SPACE eurjchem-29 45 42 2214 2214 NUM eurjchem-29 45 43     SPACE eurjchem-29 45 44 ( ( PUNCT eurjchem-29 45 45 c≡n c≡n PROPN eurjchem-29 45 46 ) ) PUNCT eurjchem-29 45 47 , , PUNCT eurjchem-29 45 48     SPACE eurjchem-29 45 49 1621 1621 NUM eurjchem-29 45 50     SPACE eurjchem-29 45 51 ( ( PUNCT eurjchem-29 45 52 c c X eurjchem-29 45 53 = = SYM eurjchem-29 45 54 c c NOUN eurjchem-29 45 55 ) ) PUNCT eurjchem-29 45 56 , , PUNCT eurjchem-29 45 57     SPACE eurjchem-29 45 58 1587 1587 NUM eurjchem-29 45 59     SPACE eurjchem-29 45 60 ( ( PUNCT eurjchem-29 45 61 c c NOUN eurjchem-29 45 62 = = SYM eurjchem-29 45 63 n n NUM eurjchem-29 45 64 ) ) PUNCT eurjchem-29 45 65 , , PUNCT eurjchem-29 45 66     SPACE eurjchem-29 45 67 721 721 NUM eurjchem-29 45 68     SPACE eurjchem-29 45 69 ( ( PUNCT eurjchem-29 45 70 c c NOUN eurjchem-29 45 71 – – PUNCT eurjchem-29 45 72 cl cl NOUN eurjchem-29 45 73 ) ) PUNCT eurjchem-29 45 74 , , PUNCT eurjchem-29 45 75     SPACE eurjchem-29 45 76 1h 1h NUM eurjchem-29 45 77     SPACE eurjchem-29 45 78 nmr nmr NOUN eurjchem-29 45 79     SPACE eurjchem-29 45 80 ( ( PUNCT eurjchem-29 45 81 200 200 NUM eurjchem-29 45 82     SPACE eurjchem-29 45 83 mhz mhz NOUN eurjchem-29 45 84 , , PUNCT eurjchem-29 45 85     SPACE eurjchem-29 45 86 dmso‐d6 dmso‐d6 NOUN eurjchem-29 45 87 ) ) PUNCT eurjchem-29 45 88 , , PUNCT eurjchem-29 45 89     SPACE eurjchem-29 45 90 δ δ PROPN eurjchem-29 45 91 : : PUNCT eurjchem-29 45 92     SPACE eurjchem-29 45 93 7.28–7.98 7.28–7.98 NUM eurjchem-29 45 94     SPACE eurjchem-29 45 95 ( ( PUNCT eurjchem-29 45 96 m m PROPN eurjchem-29 45 97 , , PUNCT eurjchem-29 45 98     SPACE eurjchem-29 45 99 15h 15h NOUN eurjchem-29 45 100 , , PUNCT eurjchem-29 45 101     SPACE eurjchem-29 45 102 ar‐h ar‐h NOUN eurjchem-29 45 103 ) ) PUNCT eurjchem-29 45 104 , , PUNCT eurjchem-29 45 105     SPACE eurjchem-29 45 106 5.71 5.71 NUM eurjchem-29 45 107     SPACE eurjchem-29 45 108 ( ( PUNCT eurjchem-29 45 109 s s PROPN eurjchem-29 45 110 , , PUNCT eurjchem-29 45 111     SPACE eurjchem-29 45 112 1h 1h NUM eurjchem-29 45 113 , , PUNCT eurjchem-29 45 114     SPACE eurjchem-29 45 115 nh nh PROPN eurjchem-29 45 116 ) ) PUNCT eurjchem-29 45 117 , , PUNCT eurjchem-29 45 118     SPACE eurjchem-29 45 119 8.71 8.71 NUM eurjchem-29 45 120     SPACE eurjchem-29 45 121 ( ( PUNCT eurjchem-29 45 122 s s PROPN eurjchem-29 45 123 , , PUNCT eurjchem-29 45 124     SPACE eurjchem-29 45 125 1h 1h NUM eurjchem-29 45 126 , , PUNCT eurjchem-29 45 127     SPACE eurjchem-29 45 128 nh nh PROPN eurjchem-29 45 129 ) ) PUNCT eurjchem-29 45 130 . . PUNCT eurjchem-29 45 131     SPACE eurjchem-29 46 1 anal anal ADJ eurjchem-29 46 2 . . PUNCT eurjchem-29 46 3     SPACE eurjchem-29 46 4 calcd calcd NOUN eurjchem-29 46 5 . . PUNCT eurjchem-29 46 6     SPACE eurjchem-29 46 7 for for ADP eurjchem-29 46 8     SPACE eurjchem-29 46 9 c28h17n6o2cl c28h17n6o2cl PROPN eurjchem-29 46 10     SPACE eurjchem-29 46 11 ( ( PUNCT eurjchem-29 46 12 504.5 504.5 NUM eurjchem-29 46 13 ): ): PUNCT eurjchem-29 46 14     SPACE eurjchem-29 46 15 c c NOUN eurjchem-29 46 16 , , PUNCT eurjchem-29 46 17     SPACE eurjchem-29 46 18 66.60 66.60 NUM eurjchem-29 46 19 ; ; PUNCT eurjchem-29 46 20     SPACE eurjchem-29 46 21 h h NOUN eurjchem-29 46 22 , , PUNCT eurjchem-29 46 23     SPACE eurjchem-29 46 24 3.36 3.36 NUM eurjchem-29 46 25 ; ; PUNCT eurjchem-29 46 26     SPACE eurjchem-29 46 27 n n CCONJ eurjchem-29 46 28 , , PUNCT eurjchem-29 46 29     SPACE eurjchem-29 46 30 16.65 16.65 NUM eurjchem-29 46 31 ; ; PUNCT eurjchem-29 46 32     SPACE eurjchem-29 46 33 cl cl NOUN eurjchem-29 46 34 , , PUNCT eurjchem-29 46 35     SPACE eurjchem-29 46 36 7.03 7.03 NUM eurjchem-29 46 37 . . PUNCT eurjchem-29 46 38     SPACE eurjchem-29 46 39 found find VERB eurjchem-29 46 40 : : PUNCT eurjchem-29 46 41     SPACE eurjchem-29 46 42 c c X eurjchem-29 46 43 , , PUNCT eurjchem-29 46 44     SPACE eurjchem-29 46 45 66.35 66.35 NUM eurjchem-29 46 46 ; ; PUNCT eurjchem-29 46 47     SPACE eurjchem-29 46 48 h h NOUN eurjchem-29 46 49 , , PUNCT eurjchem-29 46 50     SPACE eurjchem-29 46 51 3.17 3.17 NUM eurjchem-29 46 52 ; ; PUNCT eurjchem-29 46 53     SPACE eurjchem-29 46 54 n n CCONJ eurjchem-29 46 55 , , PUNCT eurjchem-29 46 56     SPACE eurjchem-29 46 57 16.29 16.29 NUM eurjchem-29 46 58 ; ; PUNCT eurjchem-29 46 59     SPACE eurjchem-29 46 60 cl cl NOUN eurjchem-29 46 61 , , PUNCT eurjchem-29 46 62     SPACE eurjchem-29 46 63 6.74 6.74 NUM eurjchem-29 46 64 % % NOUN eurjchem-29 46 65 . . PUNCT eurjchem-29 46 66       SPACE eurjchem-29 47 1 compound compound NOUN eurjchem-29 47 2     SPACE eurjchem-29 47 3 5b 5b NOUN eurjchem-29 47 4     SPACE eurjchem-29 47 5 was be AUX eurjchem-29 47 6     SPACE eurjchem-29 47 7 crystallized crystallize VERB eurjchem-29 47 8     SPACE eurjchem-29 47 9 from from ADP eurjchem-29 47 10     SPACE eurjchem-29 47 11 isopropanol isopropanol NOUN eurjchem-29 47 12 . . PUNCT eurjchem-29 47 13     SPACE eurjchem-29 47 14 yield yield NOUN eurjchem-29 47 15 : : PUNCT eurjchem-29 47 16     SPACE eurjchem-29 47 17 71 71 NUM eurjchem-29 47 18     SPACE eurjchem-29 47 19 % % NOUN eurjchem-29 47 20 . . PUNCT eurjchem-29 47 21     SPACE eurjchem-29 48 1 m.p m.p PROPN eurjchem-29 48 2 . . PROPN eurjchem-29 48 3 : : PUNCT eurjchem-29 48 4     SPACE eurjchem-29 48 5 203–205 203–205 NUM eurjchem-29 48 6     SPACE eurjchem-29 48 7 ºc ºc PROPN eurjchem-29 48 8 . . PUNCT eurjchem-29 48 9       SPACE eurjchem-29 48 10 ft‐ ft‐ AUX eurjchem-29 48 11     SPACE eurjchem-29 48 12 ir ir VERB eurjchem-29 48 13     SPACE eurjchem-29 48 14 ( ( PUNCT eurjchem-29 48 15 kbr kbr PROPN eurjchem-29 48 16 ) ) PUNCT eurjchem-29 48 17     SPACE eurjchem-29 48 18 ν ν PROPN eurjchem-29 48 19 , , PUNCT eurjchem-29 48 20     SPACE eurjchem-29 48 21 ( ( PUNCT eurjchem-29 48 22 cm‐1 cm‐1 NOUN eurjchem-29 48 23 ): ): PUNCT eurjchem-29 48 24     SPACE eurjchem-29 48 25 3354 3354 NUM eurjchem-29 48 26 , , PUNCT eurjchem-29 48 27     SPACE eurjchem-29 48 28 3276 3276 NUM eurjchem-29 48 29     SPACE eurjchem-29 48 30 ( ( PUNCT eurjchem-29 48 31 2nh 2nh PROPN eurjchem-29 48 32 ) ) PUNCT eurjchem-29 48 33 , , PUNCT eurjchem-29 48 34     SPACE eurjchem-29 48 35 1695 1695 NUM eurjchem-29 48 36     SPACE eurjchem-29 48 37 ( ( PUNCT eurjchem-29 48 38 c c NOUN eurjchem-29 48 39     SPACE eurjchem-29 48 40 = = ADJ eurjchem-29 48 41 o o NOUN eurjchem-29 48 42 ) ) PUNCT eurjchem-29 48 43 , , PUNCT eurjchem-29 48 44     SPACE eurjchem-29 48 45 2219 2219 NUM eurjchem-29 48 46     SPACE eurjchem-29 48 47 ( ( PUNCT eurjchem-29 48 48 c≡n c≡n PROPN eurjchem-29 48 49 ) ) PUNCT eurjchem-29 48 50 , , PUNCT eurjchem-29 48 51     SPACE eurjchem-29 48 52 1632 1632 NUM eurjchem-29 48 53     SPACE eurjchem-29 48 54 ( ( PUNCT eurjchem-29 48 55 c c X eurjchem-29 48 56 = = SYM eurjchem-29 48 57 c c NOUN eurjchem-29 48 58 ) ) PUNCT eurjchem-29 48 59 , , PUNCT eurjchem-29 48 60     SPACE eurjchem-29 48 61 1540 1540 NUM eurjchem-29 48 62     SPACE eurjchem-29 48 63 ( ( PUNCT eurjchem-29 48 64 c c NOUN eurjchem-29 48 65 = = SYM eurjchem-29 48 66 n n NUM eurjchem-29 48 67 ) ) PUNCT eurjchem-29 48 68 , , PUNCT eurjchem-29 48 69     SPACE eurjchem-29 48 70 727 727 NUM eurjchem-29 48 71     SPACE eurjchem-29 48 72 ( ( PUNCT eurjchem-29 48 73 c c NOUN eurjchem-29 48 74 – – PUNCT eurjchem-29 48 75 cl cl NOUN eurjchem-29 48 76 ) ) PUNCT eurjchem-29 48 77 . . PUNCT eurjchem-29 48 78     SPACE eurjchem-29 49 1 1h 1h NUM eurjchem-29 49 2     SPACE eurjchem-29 49 3 nmr nmr NOUN eurjchem-29 49 4     SPACE eurjchem-29 49 5 ( ( PUNCT eurjchem-29 49 6 200 200 NUM eurjchem-29 49 7     SPACE eurjchem-29 49 8 mhz mhz NOUN eurjchem-29 49 9 , , PUNCT eurjchem-29 49 10     SPACE eurjchem-29 49 11 dmso‐d6 dmso‐d6 NOUN eurjchem-29 49 12 ) ) PUNCT eurjchem-29 49 13 , , PUNCT eurjchem-29 49 14     SPACE eurjchem-29 49 15 δ δ PROPN eurjchem-29 49 16 : : PUNCT eurjchem-29 49 17     SPACE eurjchem-29 49 18 7.29–7.96 7.29–7.96 NUM eurjchem-29 49 19     SPACE eurjchem-29 49 20 ( ( PUNCT eurjchem-29 49 21 m m PROPN eurjchem-29 49 22 , , PUNCT eurjchem-29 49 23     SPACE eurjchem-29 49 24 15h 15h NOUN eurjchem-29 49 25 , , PUNCT eurjchem-29 49 26     SPACE eurjchem-29 49 27 ar‐h ar‐h NOUN eurjchem-29 49 28 ) ) PUNCT eurjchem-29 49 29 , , PUNCT eurjchem-29 49 30     SPACE eurjchem-29 49 31 8.83 8.83 NUM eurjchem-29 49 32     SPACE eurjchem-29 49 33 ( ( PUNCT eurjchem-29 49 34 s s PROPN eurjchem-29 49 35 , , PUNCT eurjchem-29 49 36     SPACE eurjchem-29 49 37 1h 1h NUM eurjchem-29 49 38 , , PUNCT eurjchem-29 49 39     SPACE eurjchem-29 49 40 nh nh PROPN eurjchem-29 49 41 ) ) PUNCT eurjchem-29 49 42 , , PUNCT eurjchem-29 49 43     SPACE eurjchem-29 49 44 11.23 11.23 NUM eurjchem-29 49 45     SPACE eurjchem-29 49 46 ( ( PUNCT eurjchem-29 49 47 s s PROPN eurjchem-29 49 48 , , PUNCT eurjchem-29 49 49     SPACE eurjchem-29 49 50 1h 1h NUM eurjchem-29 49 51 , , PUNCT eurjchem-29 49 52     SPACE eurjchem-29 49 53 nh nh PROPN eurjchem-29 49 54 ) ) PUNCT eurjchem-29 49 55 . . PUNCT eurjchem-29 49 56     SPACE eurjchem-29 50 1 anal anal ADJ eurjchem-29 50 2 . . PUNCT eurjchem-29 50 3     SPACE eurjchem-29 50 4 calcd calcd NOUN eurjchem-29 50 5 . . PUNCT eurjchem-29 50 6     SPACE eurjchem-29 50 7 for for ADP eurjchem-29 50 8     SPACE eurjchem-29 50 9 c28h17n7o4 c28h17n7o4 NOUN eurjchem-29 50 10     SPACE eurjchem-29 50 11 ( ( PUNCT eurjchem-29 50 12 515 515 NUM eurjchem-29 50 13 ): ): PUNCT eurjchem-29 50 14     SPACE eurjchem-29 50 15 c c NOUN eurjchem-29 50 16 , , PUNCT eurjchem-29 50 17     SPACE eurjchem-29 50 18 65.24 65.24 NUM eurjchem-29 50 19 ; ; PUNCT eurjchem-29 50 20     SPACE eurjchem-29 50 21 h h NOUN eurjchem-29 50 22 , , PUNCT eurjchem-29 50 23     SPACE eurjchem-29 50 24 3.30 3.30 NUM eurjchem-29 50 25 ; ; PUNCT eurjchem-29 50 26     SPACE eurjchem-29 50 27 n n CCONJ eurjchem-29 50 28 , , PUNCT eurjchem-29 50 29     SPACE eurjchem-29 50 30 19.02 19.02 NUM eurjchem-29 50 31 . . PUNCT eurjchem-29 50 32     SPACE eurjchem-29 50 33 found find VERB eurjchem-29 50 34 : : PUNCT eurjchem-29 50 35     SPACE eurjchem-29 50 36 c c X eurjchem-29 50 37 , , PUNCT eurjchem-29 50 38     SPACE eurjchem-29 50 39 65.69 65.69 NUM eurjchem-29 50 40 ; ; PUNCT eurjchem-29 50 41     SPACE eurjchem-29 50 42 h h NOUN eurjchem-29 50 43 , , PUNCT eurjchem-29 50 44     SPACE eurjchem-29 50 45 3.66 3.66 NUM eurjchem-29 50 46 ; ; PUNCT eurjchem-29 50 47     SPACE eurjchem-29 50 48 n n CCONJ eurjchem-29 50 49 , , PUNCT eurjchem-29 50 50     SPACE eurjchem-29 50 51 18.65 18.65 NUM eurjchem-29 50 52 % % NOUN eurjchem-29 50 53 . . PUNCT eurjchem-29 50 54           SPACE eurjchem-29 51 1 2.2.4 2.2.4 NUM eurjchem-29 51 2 . . PUNCT eurjchem-29 51 3     SPACE eurjchem-29 51 4 7­(4­chloro/3­nitrophenyl)­8­[5,6­diphenyl­4­(1,3­ 7­(4­chloro/3­nitrophenyl)­8­[5,6­diphenyl­4­(1,3­ PROPN eurjchem-29 51 5 thiazol­2­yl)­1,4­dihydro­1,2 thiazol­2­yl)­1,4­dihydro­1,2 ADJ eurjchem-29 51 6 , , PUNCT eurjchem-29 51 7     SPACE eurjchem-29 51 8 4­triazin­3­yl]­5­oxo­1,5­ 4­triazin­3­yl]­5­oxo­1,5­ PROPN eurjchem-29 51 9 dihydro[1,2,4]triazolo[1,5­a]pyridine­6­carbonitrile dihydro[1,2,4]triazolo[1,5­a]pyridine­6­carbonitrile PROPN eurjchem-29 51 10     SPACE eurjchem-29 51 11 ( ( PUNCT eurjchem-29 51 12 6a 6a NOUN eurjchem-29 51 13 , , PUNCT eurjchem-29 51 14 b b NOUN eurjchem-29 51 15 ) ) PUNCT eurjchem-29 51 16         SPACE eurjchem-29 51 17 a a DET eurjchem-29 51 18     SPACE eurjchem-29 51 19 mixture mixture NOUN eurjchem-29 51 20     SPACE eurjchem-29 51 21 of of ADP eurjchem-29 51 22     SPACE eurjchem-29 51 23 compounds compound VERB eurjchem-29 51 24     SPACE eurjchem-29 51 25 5a 5a NUM eurjchem-29 51 26 , , PUNCT eurjchem-29 51 27     SPACE eurjchem-29 51 28 b b NOUN eurjchem-29 51 29     SPACE eurjchem-29 51 30 ( ( PUNCT eurjchem-29 51 31 0.01 0.01 NUM eurjchem-29 51 32     SPACE eurjchem-29 51 33 mol mol NOUN eurjchem-29 51 34 ) ) PUNCT eurjchem-29 51 35     SPACE eurjchem-29 51 36 and and CCONJ eurjchem-29 51 37     SPACE eurjchem-29 51 38 2‐ 2‐ NUM eurjchem-29 51 39 aminothiozole aminothiozole NOUN eurjchem-29 51 40     SPACE eurjchem-29 51 41 ( ( PUNCT eurjchem-29 51 42 0.01 0.01 NUM eurjchem-29 51 43     SPACE eurjchem-29 51 44 mol mol NOUN eurjchem-29 51 45 ) ) PUNCT eurjchem-29 51 46     SPACE eurjchem-29 51 47 in in ADP eurjchem-29 51 48     SPACE eurjchem-29 51 49 absolute absolute ADJ eurjchem-29 51 50     SPACE eurjchem-29 51 51 ethanol ethanol NOUN eurjchem-29 51 52     SPACE eurjchem-29 51 53 ( ( PUNCT eurjchem-29 51 54 20 20 NUM eurjchem-29 51 55     SPACE eurjchem-29 51 56 cm3 cm3 NOUN eurjchem-29 51 57 ) ) PUNCT eurjchem-29 51 58     SPACE eurjchem-29 51 59 containing contain VERB eurjchem-29 51 60     SPACE eurjchem-29 51 61 piperidine piperidine NOUN eurjchem-29 51 62     SPACE eurjchem-29 51 63 ( ( PUNCT eurjchem-29 51 64 0.3 0.3 NUM eurjchem-29 51 65     SPACE eurjchem-29 51 66 cm3 cm3 NOUN eurjchem-29 51 67 ) ) PUNCT eurjchem-29 51 68     SPACE eurjchem-29 51 69 was be AUX eurjchem-29 51 70     SPACE eurjchem-29 51 71 heated heated ADJ eurjchem-29 51 72     SPACE eurjchem-29 51 73 under under ADP eurjchem-29 51 74     SPACE eurjchem-29 51 75 reflux reflux NOUN eurjchem-29 51 76     SPACE eurjchem-29 51 77 for for ADP eurjchem-29 51 78     SPACE eurjchem-29 51 79 5 5 NUM eurjchem-29 51 80     SPACE eurjchem-29 51 81 h h NOUN eurjchem-29 51 82     SPACE eurjchem-29 51 83 and and CCONJ eurjchem-29 51 84     SPACE eurjchem-29 51 85 then then ADV eurjchem-29 51 86     SPACE eurjchem-29 51 87 allowed allow VERB eurjchem-29 51 88     SPACE eurjchem-29 51 89 to to PART eurjchem-29 51 90     SPACE eurjchem-29 51 91 cool cool ADJ eurjchem-29 51 92 . . PUNCT eurjchem-29 51 93     SPACE eurjchem-29 52 1 the the DET eurjchem-29 52 2     SPACE eurjchem-29 52 3 precipitate precipitate NOUN eurjchem-29 52 4     SPACE eurjchem-29 52 5 that that PRON eurjchem-29 52 6     SPACE eurjchem-29 52 7 formed form VERB eurjchem-29 52 8     SPACE eurjchem-29 52 9 was be AUX eurjchem-29 52 10     SPACE eurjchem-29 52 11 filtered filter VERB eurjchem-29 52 12     SPACE eurjchem-29 52 13 off off ADP eurjchem-29 52 14 , , PUNCT eurjchem-29 52 15     SPACE eurjchem-29 52 16 dried dry VERB eurjchem-29 52 17     SPACE eurjchem-29 52 18 and and CCONJ eurjchem-29 52 19     SPACE eurjchem-29 52 20 crystallized crystallize VERB eurjchem-29 52 21     SPACE eurjchem-29 52 22 to to PART eurjchem-29 52 23     SPACE eurjchem-29 52 24 give give VERB eurjchem-29 52 25     SPACE eurjchem-29 52 26 compounds compound NOUN eurjchem-29 52 27     SPACE eurjchem-29 52 28 6a 6a NOUN eurjchem-29 52 29 , , PUNCT eurjchem-29 52 30     SPACE eurjchem-29 52 31 b b NOUN eurjchem-29 52 32 , , PUNCT eurjchem-29 52 33     SPACE eurjchem-29 52 34 respectively respectively ADV eurjchem-29 52 35     SPACE eurjchem-29 52 36 ( ( PUNCT eurjchem-29 52 37 scheme scheme NOUN eurjchem-29 52 38     SPACE eurjchem-29 52 39 1 1 NUM eurjchem-29 52 40 ) ) PUNCT eurjchem-29 52 41 . . PUNCT eurjchem-29 52 42     SPACE eurjchem-29 53 1 compound compound NOUN eurjchem-29 53 2     SPACE eurjchem-29 53 3 6a 6a NOUN eurjchem-29 53 4     SPACE eurjchem-29 53 5 was be AUX eurjchem-29 53 6     SPACE eurjchem-29 53 7 crystallized crystallize VERB eurjchem-29 53 8     SPACE eurjchem-29 53 9 from from ADP eurjchem-29 53 10     SPACE eurjchem-29 53 11 ethanol ethanol NOUN eurjchem-29 53 12 . . PUNCT eurjchem-29 53 13     SPACE eurjchem-29 53 14 yield yield NOUN eurjchem-29 53 15 : : PUNCT eurjchem-29 53 16     SPACE eurjchem-29 53 17 56 56 NUM eurjchem-29 53 18 % % NOUN eurjchem-29 53 19 . . PUNCT eurjchem-29 53 20     SPACE eurjchem-29 54 1 m.p m.p PROPN eurjchem-29 54 2 . . PROPN eurjchem-29 54 3 : : PUNCT eurjchem-29 54 4     SPACE eurjchem-29 54 5 194‐196 194‐196 NUM eurjchem-29 54 6     SPACE eurjchem-29 54 7 ºc ºc PROPN eurjchem-29 54 8 . . PUNCT eurjchem-29 54 9     SPACE eurjchem-29 54 10 ft‐ ft‐ PROPN eurjchem-29 54 11     SPACE eurjchem-29 54 12 ir ir PROPN eurjchem-29 54 13     SPACE eurjchem-29 54 14 ( ( PUNCT eurjchem-29 54 15 kbr kbr PROPN eurjchem-29 54 16 ) ) PUNCT eurjchem-29 54 17     SPACE eurjchem-29 54 18 ν ν NOUN eurjchem-29 54 19 , , PUNCT eurjchem-29 54 20     SPACE eurjchem-29 54 21 ( ( PUNCT eurjchem-29 54 22 cm‐1 cm‐1 NOUN eurjchem-29 54 23 ): ): PUNCT eurjchem-29 54 24     SPACE eurjchem-29 54 25 3383 3383 NUM eurjchem-29 54 26 , , PUNCT eurjchem-29 54 27     SPACE eurjchem-29 54 28 3263 3263 NUM eurjchem-29 54 29     SPACE eurjchem-29 54 30 ( ( PUNCT eurjchem-29 54 31 2nh 2nh PROPN eurjchem-29 54 32 ) ) PUNCT eurjchem-29 54 33 , , PUNCT eurjchem-29 54 34     SPACE eurjchem-29 54 35 2213 2213 NUM eurjchem-29 54 36     SPACE eurjchem-29 54 37 ( ( PUNCT eurjchem-29 54 38 c≡n c≡n PROPN eurjchem-29 54 39 ) ) PUNCT eurjchem-29 54 40 , , PUNCT eurjchem-29 54 41     SPACE eurjchem-29 54 42 1688 1688 NUM eurjchem-29 54 43     SPACE eurjchem-29 54 44 ( ( PUNCT eurjchem-29 54 45 c c NOUN eurjchem-29 54 46 = = NOUN eurjchem-29 54 47 o o NOUN eurjchem-29 54 48 ) ) PUNCT eurjchem-29 54 49 , , PUNCT eurjchem-29 54 50     SPACE eurjchem-29 54 51 1597(c 1597(c NOUN eurjchem-29 54 52 = = NOUN eurjchem-29 54 53 n n CCONJ eurjchem-29 54 54 ) ) PUNCT eurjchem-29 54 55 , , PUNCT eurjchem-29 54 56     SPACE eurjchem-29 54 57 791 791 NUM eurjchem-29 54 58     SPACE eurjchem-29 54 59 ( ( PUNCT eurjchem-29 54 60 c c NOUN eurjchem-29 54 61 – – PUNCT eurjchem-29 54 62 cl cl NOUN eurjchem-29 54 63 ) ) PUNCT eurjchem-29 54 64 . . PUNCT eurjchem-29 54 65     SPACE eurjchem-29 55 1 1h 1h NUM eurjchem-29 55 2     SPACE eurjchem-29 55 3 nmr nmr NOUN eurjchem-29 55 4     SPACE eurjchem-29 55 5 ( ( PUNCT eurjchem-29 55 6 200 200 NUM eurjchem-29 55 7     SPACE eurjchem-29 55 8 mhz mhz NOUN eurjchem-29 55 9 , , PUNCT eurjchem-29 55 10     SPACE eurjchem-29 55 11 dmso‐d6 dmso‐d6 NOUN eurjchem-29 55 12 ) ) PUNCT eurjchem-29 55 13 , , PUNCT eurjchem-29 55 14     SPACE eurjchem-29 55 15 δ δ PROPN eurjchem-29 55 16 : : PUNCT eurjchem-29 55 17     SPACE eurjchem-29 55 18 7.41–7.62 7.41–7.62 NUM eurjchem-29 55 19     SPACE eurjchem-29 55 20 ( ( PUNCT eurjchem-29 55 21 m m PROPN eurjchem-29 55 22 , , PUNCT eurjchem-29 55 23     SPACE eurjchem-29 55 24 17h 17h NOUN eurjchem-29 55 25 , , PUNCT eurjchem-29 55 26     SPACE eurjchem-29 55 27 ar‐h ar‐h NOUN eurjchem-29 55 28 ) ) PUNCT eurjchem-29 55 29 , , PUNCT eurjchem-29 55 30     SPACE eurjchem-29 55 31 6.08 6.08 NUM eurjchem-29 55 32     SPACE eurjchem-29 55 33 ( ( PUNCT eurjchem-29 55 34 s s PROPN eurjchem-29 55 35 , , PUNCT eurjchem-29 55 36     SPACE eurjchem-29 55 37 1h 1h NUM eurjchem-29 55 38 , , PUNCT eurjchem-29 55 39     SPACE eurjchem-29 55 40 nh nh PROPN eurjchem-29 55 41 ) ) PUNCT eurjchem-29 55 42 , , PUNCT eurjchem-29 55 43     SPACE eurjchem-29 55 44 8.73 8.73 NUM eurjchem-29 55 45     SPACE eurjchem-29 55 46 ( ( PUNCT eurjchem-29 55 47 s s PROPN eurjchem-29 55 48 , , PUNCT eurjchem-29 55 49     SPACE eurjchem-29 55 50 1h 1h NUM eurjchem-29 55 51 , , PUNCT eurjchem-29 55 52     SPACE eurjchem-29 55 53 nh nh PROPN eurjchem-29 55 54 ) ) PUNCT eurjchem-29 55 55 . . PUNCT eurjchem-29 55 56     SPACE eurjchem-29 56 1 anal anal ADJ eurjchem-29 56 2 . . PUNCT eurjchem-29 56 3     SPACE eurjchem-29 56 4 calcd calcd NOUN eurjchem-29 56 5 . . PUNCT eurjchem-29 56 6     SPACE eurjchem-29 57 1 for for ADP eurjchem-29 57 2     SPACE eurjchem-29 57 3 c31h19n8oscl c31h19n8oscl PROPN eurjchem-29 57 4     SPACE eurjchem-29 57 5 ( ( PUNCT eurjchem-29 57 6 586.5 586.5 NUM eurjchem-29 57 7 ): ): PUNCT eurjchem-29 57 8     SPACE eurjchem-29 57 9 c c NOUN eurjchem-29 57 10 , , PUNCT eurjchem-29 57 11     SPACE eurjchem-29 57 12 63.42 63.42 NUM eurjchem-29 57 13 ; ; PUNCT eurjchem-29 57 14     SPACE eurjchem-29 57 15 h h NOUN eurjchem-29 57 16 , , PUNCT eurjchem-29 57 17     SPACE eurjchem-29 57 18 3.23 3.23 NUM eurjchem-29 57 19 ; ; PUNCT eurjchem-29 57 20     SPACE eurjchem-29 57 21 n n CCONJ eurjchem-29 57 22 , , PUNCT eurjchem-29 57 23     SPACE eurjchem-29 57 24 19.09 19.09 NUM eurjchem-29 57 25 ; ; PUNCT eurjchem-29 57 26     SPACE eurjchem-29 57 27 s s PROPN eurjchem-29 57 28 , , PUNCT eurjchem-29 57 29     SPACE eurjchem-29 57 30 5.45 5.45 NUM eurjchem-29 57 31 ; ; PUNCT eurjchem-29 57 32     SPACE eurjchem-29 57 33 cl cl NOUN eurjchem-29 57 34 , , PUNCT eurjchem-29 57 35     SPACE eurjchem-29 57 36 6.05 6.05 NUM eurjchem-29 57 37 . . PUNCT eurjchem-29 57 38     SPACE eurjchem-29 57 39 found find VERB eurjchem-29 57 40 : : PUNCT eurjchem-29 57 41     SPACE eurjchem-29 57 42 c c X eurjchem-29 57 43 , , PUNCT eurjchem-29 57 44     SPACE eurjchem-29 57 45 63.05 63.05 NUM eurjchem-29 57 46 ; ; PUNCT eurjchem-29 57 47     SPACE eurjchem-29 57 48 h h NOUN eurjchem-29 57 49 , , PUNCT eurjchem-29 57 50     SPACE eurjchem-29 57 51 2.91 2.91 NUM eurjchem-29 57 52 ; ; PUNCT eurjchem-29 57 53     SPACE eurjchem-29 57 54 n n CCONJ eurjchem-29 57 55 , , PUNCT eurjchem-29 57 56     SPACE eurjchem-29 57 57 18.75 18.75 NUM eurjchem-29 57 58 ; ; PUNCT eurjchem-29 57 59     SPACE eurjchem-29 57 60 s s PROPN eurjchem-29 57 61 , , PUNCT eurjchem-29 57 62     SPACE eurjchem-29 57 63 5.12 5.12 NUM eurjchem-29 57 64 ; ; PUNCT eurjchem-29 57 65     SPACE eurjchem-29 57 66 cl cl NOUN eurjchem-29 57 67 , , PUNCT eurjchem-29 57 68     SPACE eurjchem-29 57 69 6.16 6.16 NUM eurjchem-29 57 70 % % NOUN eurjchem-29 57 71 . . PUNCT eurjchem-29 57 72       SPACE eurjchem-29 57 73 compound compound NOUN eurjchem-29 57 74     SPACE eurjchem-29 57 75 6b 6b NOUN eurjchem-29 57 76     SPACE eurjchem-29 57 77 was be AUX eurjchem-29 57 78     SPACE eurjchem-29 57 79 crystallized crystallize VERB eurjchem-29 57 80     SPACE eurjchem-29 57 81 from from ADP eurjchem-29 57 82     SPACE eurjchem-29 57 83 isopropanol isopropanol NOUN eurjchem-29 57 84 . . PUNCT eurjchem-29 57 85     SPACE eurjchem-29 57 86 yield yield NOUN eurjchem-29 57 87 : : PUNCT eurjchem-29 57 88     SPACE eurjchem-29 57 89 64 64 NUM eurjchem-29 57 90     SPACE eurjchem-29 57 91 % % NOUN eurjchem-29 57 92 . . PUNCT eurjchem-29 57 93     SPACE eurjchem-29 58 1 m.p m.p PROPN eurjchem-29 58 2 . . PROPN eurjchem-29 58 3 : : PUNCT eurjchem-29 58 4     SPACE eurjchem-29 58 5 187‐188 187‐188 NUM eurjchem-29 58 6     SPACE eurjchem-29 58 7 ° ° PROPN eurjchem-29 58 8 c c NOUN eurjchem-29 58 9 . . PUNCT eurjchem-29 58 10     SPACE eurjchem-29 59 1 ft‐ ft‐ VERB eurjchem-29 59 2     SPACE eurjchem-29 59 3 ir ir VERB eurjchem-29 59 4     SPACE eurjchem-29 59 5 ( ( PUNCT eurjchem-29 59 6 kbr kbr PROPN eurjchem-29 59 7 ) ) PUNCT eurjchem-29 59 8     SPACE eurjchem-29 59 9 ν ν PROPN eurjchem-29 59 10 , , PUNCT eurjchem-29 59 11     SPACE eurjchem-29 59 12 ( ( PUNCT eurjchem-29 59 13 cm‐1 cm‐1 NOUN eurjchem-29 59 14 ): ): PUNCT eurjchem-29 59 15       SPACE eurjchem-29 59 16 3374 3374 NUM eurjchem-29 59 17 , , PUNCT eurjchem-29 59 18     SPACE eurjchem-29 59 19 3263 3263 NUM eurjchem-29 59 20     SPACE eurjchem-29 59 21 ( ( PUNCT eurjchem-29 59 22 2nh 2nh PROPN eurjchem-29 59 23 ) ) PUNCT eurjchem-29 59 24 , , PUNCT eurjchem-29 59 25     SPACE eurjchem-29 59 26 2216 2216 NUM eurjchem-29 59 27     SPACE eurjchem-29 59 28 ( ( PUNCT eurjchem-29 59 29 c≡n c≡n PROPN eurjchem-29 59 30 ) ) PUNCT eurjchem-29 59 31 , , PUNCT eurjchem-29 59 32     SPACE eurjchem-29 59 33 1687 1687 NUM eurjchem-29 59 34     SPACE eurjchem-29 59 35 ( ( PUNCT eurjchem-29 59 36 c c NOUN eurjchem-29 59 37 = = NOUN eurjchem-29 59 38 o o NOUN eurjchem-29 59 39 ) ) PUNCT eurjchem-29 59 40 , , PUNCT eurjchem-29 59 41     SPACE eurjchem-29 59 42 1567 1567 NUM eurjchem-29 59 43     SPACE eurjchem-29 59 44 ( ( PUNCT eurjchem-29 59 45 c c NOUN eurjchem-29 59 46 = = SYM eurjchem-29 59 47 n n NUM eurjchem-29 59 48 ) ) PUNCT eurjchem-29 59 49 . . PUNCT eurjchem-29 59 50         SPACE eurjchem-29 60 1 1h 1h NUM eurjchem-29 60 2     SPACE eurjchem-29 60 3 nmr nmr NOUN eurjchem-29 60 4     SPACE eurjchem-29 60 5 ( ( PUNCT eurjchem-29 60 6 200 200 NUM eurjchem-29 60 7     SPACE eurjchem-29 60 8 mhz mhz NOUN eurjchem-29 60 9 , , PUNCT eurjchem-29 60 10     SPACE eurjchem-29 60 11 dmso‐d6 dmso‐d6 NOUN eurjchem-29 60 12 ) ) PUNCT eurjchem-29 60 13 , , PUNCT eurjchem-29 60 14     SPACE eurjchem-29 60 15 δ δ PROPN eurjchem-29 60 16 : : PUNCT eurjchem-29 60 17     SPACE eurjchem-29 60 18 7.21–7.98 7.21–7.98 NUM eurjchem-29 60 19     SPACE eurjchem-29 60 20 ( ( PUNCT eurjchem-29 60 21 m m PROPN eurjchem-29 60 22 , , PUNCT eurjchem-29 60 23     SPACE eurjchem-29 60 24 17h 17h NOUN eurjchem-29 60 25 , , PUNCT eurjchem-29 60 26     SPACE eurjchem-29 60 27 ar‐h ar‐h NOUN eurjchem-29 60 28 ) ) PUNCT eurjchem-29 60 29 , , PUNCT eurjchem-29 60 30     SPACE eurjchem-29 60 31 6.49 6.49 NUM eurjchem-29 60 32     SPACE eurjchem-29 60 33 ( ( PUNCT eurjchem-29 60 34 s s PROPN eurjchem-29 60 35 , , PUNCT eurjchem-29 60 36     SPACE eurjchem-29 60 37 1h 1h NUM eurjchem-29 60 38 , , PUNCT eurjchem-29 60 39     SPACE eurjchem-29 60 40 nh nh PROPN eurjchem-29 60 41 ) ) PUNCT eurjchem-29 60 42 , , PUNCT eurjchem-29 60 43     SPACE eurjchem-29 60 44 8.67 8.67 NUM eurjchem-29 60 45     SPACE eurjchem-29 60 46 ( ( PUNCT eurjchem-29 60 47 s s PROPN eurjchem-29 60 48 , , PUNCT eurjchem-29 60 49     SPACE eurjchem-29 60 50 1h 1h NUM eurjchem-29 60 51 , , PUNCT eurjchem-29 60 52     SPACE eurjchem-29 60 53 nh nh PROPN eurjchem-29 60 54 ) ) PUNCT eurjchem-29 60 55 . . PUNCT eurjchem-29 60 56     SPACE eurjchem-29 61 1 ms ms PROPN eurjchem-29 61 2     SPACE eurjchem-29 61 3 ( ( PUNCT eurjchem-29 61 4 m m PROPN eurjchem-29 61 5 / / SYM eurjchem-29 61 6 z z NOUN eurjchem-29 61 7 , , PUNCT eurjchem-29 61 8     SPACE eurjchem-29 61 9 i i PRON eurjchem-29 61 10     SPACE eurjchem-29 61 11 % % VERB eurjchem-29 61 12 ): ): PUNCT eurjchem-29 61 13     SPACE eurjchem-29 61 14 599 599 NUM eurjchem-29 61 15     SPACE eurjchem-29 61 16 ( ( PUNCT eurjchem-29 61 17 m+2 m+2 NOUN eurjchem-29 61 18 , , PUNCT eurjchem-29 61 19     SPACE eurjchem-29 61 20 6 6 NUM eurjchem-29 61 21 % % NOUN eurjchem-29 61 22 ) ) PUNCT eurjchem-29 61 23 , , PUNCT eurjchem-29 61 24     SPACE eurjchem-29 61 25 443 443 NUM eurjchem-29 61 26     SPACE eurjchem-29 61 27 ( ( PUNCT eurjchem-29 61 28 4 4 NUM eurjchem-29 61 29 ) ) PUNCT eurjchem-29 61 30 , , PUNCT eurjchem-29 61 31     SPACE eurjchem-29 61 32 321 321 NUM eurjchem-29 61 33     SPACE eurjchem-29 61 34 ( ( PUNCT eurjchem-29 61 35 17 17 NUM eurjchem-29 61 36 ) ) PUNCT eurjchem-29 61 37 , , PUNCT eurjchem-29 61 38     SPACE eurjchem-29 61 39 293 293 NUM eurjchem-29 61 40     SPACE eurjchem-29 61 41 ( ( PUNCT eurjchem-29 61 42 7 7 NUM eurjchem-29 61 43 ) ) PUNCT eurjchem-29 61 44 , , PUNCT eurjchem-29 61 45     SPACE eurjchem-29 61 46 235 235 NUM eurjchem-29 61 47     SPACE eurjchem-29 61 48 ( ( PUNCT eurjchem-29 61 49 13 13 NUM eurjchem-29 61 50 ) ) PUNCT eurjchem-29 61 51 , , PUNCT eurjchem-29 61 52     SPACE eurjchem-29 61 53 216 216 NUM eurjchem-29 61 54     SPACE eurjchem-29 61 55 ( ( PUNCT eurjchem-29 61 56 6 6 NUM eurjchem-29 61 57 ) ) PUNCT eurjchem-29 61 58 , , PUNCT eurjchem-29 61 59     SPACE eurjchem-29 61 60 206 206 NUM eurjchem-29 61 61     SPACE eurjchem-29 61 62 ( ( PUNCT eurjchem-29 61 63 10 10 NUM eurjchem-29 61 64 ) ) PUNCT eurjchem-29 61 65 , , PUNCT eurjchem-29 61 66     SPACE eurjchem-29 61 67 192 192 NUM eurjchem-29 61 68     SPACE eurjchem-29 61 69 ( ( PUNCT eurjchem-29 61 70 13 13 NUM eurjchem-29 61 71 ) ) PUNCT eurjchem-29 61 72 , , PUNCT eurjchem-29 61 73     SPACE eurjchem-29 61 74 165 165 NUM eurjchem-29 61 75     SPACE eurjchem-29 61 76 ( ( PUNCT eurjchem-29 61 77 17 17 NUM eurjchem-29 61 78 ) ) PUNCT eurjchem-29 61 79 , , PUNCT eurjchem-29 61 80     SPACE eurjchem-29 61 81 164 164 NUM eurjchem-29 61 82     SPACE eurjchem-29 61 83 ( ( PUNCT eurjchem-29 61 84 12 12 NUM eurjchem-29 61 85 ) ) PUNCT eurjchem-29 61 86 , , PUNCT eurjchem-29 61 87     SPACE eurjchem-29 61 88 115 115 NUM eurjchem-29 61 89     SPACE eurjchem-29 61 90 ( ( PUNCT eurjchem-29 61 91 13 13 NUM eurjchem-29 61 92 ) ) PUNCT eurjchem-29 61 93 , , PUNCT eurjchem-29 61 94     SPACE eurjchem-29 61 95 105 105 NUM eurjchem-29 61 96     SPACE eurjchem-29 61 97 ( ( PUNCT eurjchem-29 61 98 100 100 NUM eurjchem-29 61 99 ) ) PUNCT eurjchem-29 61 100 , , PUNCT eurjchem-29 61 101     SPACE eurjchem-29 61 102 57 57 NUM eurjchem-29 61 103     SPACE eurjchem-29 61 104 ( ( PUNCT eurjchem-29 61 105 14 14 NUM eurjchem-29 61 106 ) ) PUNCT eurjchem-29 61 107 . . PUNCT eurjchem-29 61 108     SPACE eurjchem-29 62 1 anal anal ADJ eurjchem-29 62 2 . . PUNCT eurjchem-29 62 3     SPACE eurjchem-29 62 4 calcd calcd NOUN eurjchem-29 62 5 . . PUNCT eurjchem-29 62 6     SPACE eurjchem-29 62 7 for for ADP eurjchem-29 62 8     SPACE eurjchem-29 62 9 c31h19n9o3s c31h19n9o3 NOUN eurjchem-29 62 10     SPACE eurjchem-29 62 11 ( ( PUNCT eurjchem-29 62 12 597 597 NUM eurjchem-29 62 13 ): ): PUNCT eurjchem-29 62 14     SPACE eurjchem-29 62 15 c c NOUN eurjchem-29 62 16 , , PUNCT eurjchem-29 62 17     SPACE eurjchem-29 62 18 62.31 62.31 NUM eurjchem-29 62 19 ; ; PUNCT eurjchem-29 62 20     SPACE eurjchem-29 62 21 h h NOUN eurjchem-29 62 22 , , PUNCT eurjchem-29 62 23     SPACE eurjchem-29 62 24 3.18 3.18 NUM eurjchem-29 62 25 ; ; PUNCT eurjchem-29 62 26     SPACE eurjchem-29 62 27 n n CCONJ eurjchem-29 62 28 , , PUNCT eurjchem-29 62 29     SPACE eurjchem-29 62 30 21.10 21.10 NUM eurjchem-29 62 31 ; ; PUNCT eurjchem-29 62 32     SPACE eurjchem-29 62 33 s s PROPN eurjchem-29 62 34 , , PUNCT eurjchem-29 62 35     SPACE eurjchem-29 62 36 5.36 5.36 NUM eurjchem-29 62 37 . . PUNCT eurjchem-29 62 38     SPACE eurjchem-29 62 39 found find VERB eurjchem-29 62 40 : : PUNCT eurjchem-29 62 41     SPACE eurjchem-29 62 42 c c X eurjchem-29 62 43 , , PUNCT eurjchem-29 62 44     SPACE eurjchem-29 62 45 61.97 61.97 NUM eurjchem-29 62 46 ; ; PUNCT eurjchem-29 62 47     SPACE eurjchem-29 62 48 h h NOUN eurjchem-29 62 49 , , PUNCT eurjchem-29 62 50     SPACE eurjchem-29 62 51 2.89 2.89 NUM eurjchem-29 62 52 ; ; PUNCT eurjchem-29 62 53     SPACE eurjchem-29 62 54 n n CCONJ eurjchem-29 62 55 , , PUNCT eurjchem-29 62 56     SPACE eurjchem-29 62 57 20.76 20.76 NUM eurjchem-29 62 58 ; ; PUNCT eurjchem-29 62 59     SPACE eurjchem-29 62 60 s s PROPN eurjchem-29 62 61 , , PUNCT eurjchem-29 62 62     SPACE eurjchem-29 62 63 5.11 5.11 NUM eurjchem-29 62 64 % % NOUN eurjchem-29 62 65 . . PUNCT eurjchem-29 62 66           SPACE eurjchem-29 62 67 2.2.5 2.2.5 NUM eurjchem-29 62 68 . . PUNCT eurjchem-29 62 69     SPACE eurjchem-29 63 1 8­[5,6­diphenyl­4­(1,3­thiazol­2­yl)­1h­1,2,4­triazin­3­ 8­[5,6­diphenyl­4­(1,3­thiazol­2­yl)­1h­1,2,4­triazin­3­ PROPN eurjchem-29 63 2 yl]­7­(3­nitrophenyl)­5­oxo­1­(chloroacetyl)[1,2,4]triazolo yl]­7­(3­nitrophenyl)­5­oxo­1­(chloroacetyl)[1,2,4]triazolo NOUN eurjchem-29 63 3     SPACE eurjchem-29 64 1 [ [ X eurjchem-29 64 2 1,5­a]pyridine­6­carbonitrile 1,5­a]pyridine­6­carbonitrile NUM eurjchem-29 64 3     SPACE eurjchem-29 64 4 ( ( PUNCT eurjchem-29 64 5 7 7 NUM eurjchem-29 64 6 ) ) PUNCT eurjchem-29 64 7         SPACE eurjchem-29 64 8 an an DET eurjchem-29 64 9     SPACE eurjchem-29 64 10 equimolar equimolar NOUN eurjchem-29 64 11     SPACE eurjchem-29 64 12 mixture mixture NOUN eurjchem-29 64 13     SPACE eurjchem-29 64 14 of of ADP eurjchem-29 64 15     SPACE eurjchem-29 64 16 compound compound NOUN eurjchem-29 64 17     SPACE eurjchem-29 64 18 6b 6b NOUN eurjchem-29 64 19     SPACE eurjchem-29 64 20 ( ( PUNCT eurjchem-29 64 21 0.01 0.01 NUM eurjchem-29 64 22     SPACE eurjchem-29 64 23 mol mol NOUN eurjchem-29 64 24 ) ) PUNCT eurjchem-29 64 25     SPACE eurjchem-29 64 26 and and CCONJ eurjchem-29 64 27     SPACE eurjchem-29 64 28 chloroacetyl chloroacetyl NOUN eurjchem-29 64 29     SPACE eurjchem-29 64 30 chloride chloride NOUN eurjchem-29 64 31     SPACE eurjchem-29 64 32 ( ( PUNCT eurjchem-29 64 33 0.01 0.01 NUM eurjchem-29 64 34     SPACE eurjchem-29 64 35 mol mol NOUN eurjchem-29 64 36 ) ) PUNCT eurjchem-29 64 37     SPACE eurjchem-29 64 38 in in ADP eurjchem-29 64 39     SPACE eurjchem-29 64 40 dmf dmf PROPN eurjchem-29 64 41     SPACE eurjchem-29 64 42 ( ( PUNCT eurjchem-29 64 43 20 20 NUM eurjchem-29 64 44     SPACE eurjchem-29 64 45 cm3 cm3 NOUN eurjchem-29 64 46 ) ) PUNCT eurjchem-29 64 47     SPACE eurjchem-29 64 48 was be AUX eurjchem-29 64 49     SPACE eurjchem-29 64 50 refluxed refluxe VERB eurjchem-29 64 51     SPACE eurjchem-29 64 52 for for ADP eurjchem-29 64 53     SPACE eurjchem-29 64 54 2h 2h NUM eurjchem-29 64 55 , , PUNCT eurjchem-29 64 56     SPACE eurjchem-29 64 57 and and CCONJ eurjchem-29 64 58     SPACE eurjchem-29 64 59 then then ADV eurjchem-29 64 60     SPACE eurjchem-29 64 61 allowed allow VERB eurjchem-29 64 62     SPACE eurjchem-29 64 63 to to PART eurjchem-29 64 64     SPACE eurjchem-29 64 65 cool cool ADJ eurjchem-29 64 66 . . PUNCT eurjchem-29 64 67     SPACE eurjchem-29 65 1 the the DET eurjchem-29 65 2     SPACE eurjchem-29 65 3 reaction reaction NOUN eurjchem-29 65 4     SPACE eurjchem-29 65 5 mixture mixture NOUN eurjchem-29 65 6     SPACE eurjchem-29 65 7 was be AUX eurjchem-29 65 8     SPACE eurjchem-29 65 9 poured pour VERB eurjchem-29 65 10     SPACE eurjchem-29 65 11 onto onto ADP eurjchem-29 65 12     SPACE eurjchem-29 65 13 ice ice NOUN eurjchem-29 65 14     SPACE eurjchem-29 65 15 water water NOUN eurjchem-29 65 16 . . PUNCT eurjchem-29 65 17     SPACE eurjchem-29 66 1 the the DET eurjchem-29 66 2     SPACE eurjchem-29 66 3 solid solid ADJ eurjchem-29 66 4     SPACE eurjchem-29 66 5 product product NOUN eurjchem-29 66 6     SPACE eurjchem-29 66 7 that that PRON eurjchem-29 66 8     SPACE eurjchem-29 66 9 formed form VERB eurjchem-29 66 10     SPACE eurjchem-29 66 11 was be AUX eurjchem-29 66 12     SPACE eurjchem-29 66 13 filtered filter VERB eurjchem-29 66 14     SPACE eurjchem-29 66 15 off off ADP eurjchem-29 66 16 , , PUNCT eurjchem-29 66 17     SPACE eurjchem-29 66 18 dried dry VERB eurjchem-29 66 19     SPACE eurjchem-29 66 20 and and CCONJ eurjchem-29 66 21     SPACE eurjchem-29 66 22 crystallized crystallize VERB eurjchem-29 66 23     SPACE eurjchem-29 66 24 from from ADP eurjchem-29 66 25     SPACE eurjchem-29 66 26 a a DET eurjchem-29 66 27     SPACE eurjchem-29 66 28 mixture mixture NOUN eurjchem-29 66 29     SPACE eurjchem-29 66 30 of of ADP eurjchem-29 66 31     SPACE eurjchem-29 66 32 methanol methanol NOUN eurjchem-29 66 33     SPACE eurjchem-29 66 34 and and CCONJ eurjchem-29 66 35     SPACE eurjchem-29 66 36 water water NOUN eurjchem-29 66 37     SPACE eurjchem-29 66 38 ( ( PUNCT eurjchem-29 66 39 1:1 1:1 NUM eurjchem-29 66 40 ) ) PUNCT eurjchem-29 66 41     SPACE eurjchem-29 66 42 ( ( PUNCT eurjchem-29 66 43 scheme scheme NOUN eurjchem-29 66 44     SPACE eurjchem-29 66 45 2 2 NUM eurjchem-29 66 46 ) ) PUNCT eurjchem-29 66 47     SPACE eurjchem-29 66 48 .yield .yield PROPN eurjchem-29 66 49 : : PUNCT eurjchem-29 66 50     SPACE eurjchem-29 66 51 80 80 NUM eurjchem-29 66 52 % % NOUN eurjchem-29 66 53 . . PUNCT eurjchem-29 66 54     SPACE eurjchem-29 67 1 m.p m.p PROPN eurjchem-29 67 2 . . PROPN eurjchem-29 67 3 : : PUNCT eurjchem-29 67 4     SPACE eurjchem-29 67 5 252‐255 252‐255 NUM eurjchem-29 67 6     SPACE eurjchem-29 67 7 ° ° PROPN eurjchem-29 67 8 c c NOUN eurjchem-29 67 9 . . PUNCT eurjchem-29 67 10     SPACE eurjchem-29 68 1 ft‐ ft‐ PROPN eurjchem-29 68 2     SPACE eurjchem-29 68 3 ir ir PROPN eurjchem-29 68 4     SPACE eurjchem-29 68 5 ( ( PUNCT eurjchem-29 68 6 kbr kbr PROPN eurjchem-29 68 7 ) ) PUNCT eurjchem-29 68 8     SPACE eurjchem-29 68 9 ν ν NOUN eurjchem-29 68 10 , , PUNCT eurjchem-29 68 11     SPACE eurjchem-29 68 12 ( ( PUNCT eurjchem-29 68 13 cm‐1 cm‐1 NOUN eurjchem-29 68 14 ): ): PUNCT eurjchem-29 68 15     SPACE eurjchem-29 68 16 3265 3265 NUM eurjchem-29 68 17     SPACE eurjchem-29 68 18 ( ( PUNCT eurjchem-29 68 19 nh nh NOUN eurjchem-29 68 20 ) ) PUNCT eurjchem-29 68 21 , , PUNCT eurjchem-29 68 22     SPACE eurjchem-29 68 23 2985 2985 NUM eurjchem-29 68 24     SPACE eurjchem-29 68 25 ( ( PUNCT eurjchem-29 68 26 ch2 ch2 PROPN eurjchem-29 68 27 ) ) PUNCT eurjchem-29 68 28 , , PUNCT eurjchem-29 68 29     SPACE eurjchem-29 68 30 2214 2214 NUM eurjchem-29 68 31     SPACE eurjchem-29 68 32 ( ( PUNCT eurjchem-29 68 33 c≡n c≡n PROPN eurjchem-29 68 34 ) ) PUNCT eurjchem-29 68 35 , , PUNCT eurjchem-29 68 36     SPACE eurjchem-29 68 37 1654 1654 NUM eurjchem-29 68 38 , , PUNCT eurjchem-29 68 39     SPACE eurjchem-29 68 40 1686 1686 NUM eurjchem-29 68 41     SPACE eurjchem-29 68 42 ( ( PUNCT eurjchem-29 68 43 2c 2c NOUN eurjchem-29 68 44 = = SYM eurjchem-29 68 45 o o NOUN eurjchem-29 68 46 ) ) PUNCT eurjchem-29 68 47 , , PUNCT eurjchem-29 68 48     SPACE eurjchem-29 68 49 1594 1594 NUM eurjchem-29 68 50     SPACE eurjchem-29 68 51 ( ( PUNCT eurjchem-29 68 52 c c NOUN eurjchem-29 68 53 = = SYM eurjchem-29 68 54 n n NUM eurjchem-29 68 55 ) ) PUNCT eurjchem-29 68 56 . . PUNCT eurjchem-29 68 57     SPACE eurjchem-29 69 1 1h 1h NUM eurjchem-29 69 2     SPACE eurjchem-29 69 3 nmr nmr NOUN eurjchem-29 69 4     SPACE eurjchem-29 69 5 ( ( PUNCT eurjchem-29 69 6 200 200 NUM eurjchem-29 69 7     SPACE eurjchem-29 69 8 mhz mhz NOUN eurjchem-29 69 9 , , PUNCT eurjchem-29 69 10     SPACE eurjchem-29 69 11 dmso‐d6 dmso‐d6 NOUN eurjchem-29 69 12 ) ) PUNCT eurjchem-29 69 13 , , PUNCT eurjchem-29 69 14     SPACE eurjchem-29 69 15 δ δ PROPN eurjchem-29 69 16 : : PUNCT eurjchem-29 69 17     SPACE eurjchem-29 69 18 2.89 2.89 NUM eurjchem-29 69 19     SPACE eurjchem-29 69 20 ( ( PUNCT eurjchem-29 69 21 s s PROPN eurjchem-29 69 22 , , PUNCT eurjchem-29 69 23     SPACE eurjchem-29 69 24 2h 2h NUM eurjchem-29 69 25 , , PUNCT eurjchem-29 69 26     SPACE eurjchem-29 69 27 ch2 ch2 NOUN eurjchem-29 69 28 ) ) PUNCT eurjchem-29 69 29 , , PUNCT eurjchem-29 69 30     SPACE eurjchem-29 69 31 7.52‐8.3 7.52‐8.3 NUM eurjchem-29 69 32 , , PUNCT eurjchem-29 69 33     SPACE eurjchem-29 69 34 ( ( PUNCT eurjchem-29 69 35 m m PROPN eurjchem-29 69 36 , , PUNCT eurjchem-29 69 37     SPACE eurjchem-29 69 38 17h 17h NOUN eurjchem-29 69 39 , , PUNCT eurjchem-29 69 40     SPACE eurjchem-29 69 41 ar‐h ar‐h NOUN eurjchem-29 69 42 ) ) PUNCT eurjchem-29 69 43 , , PUNCT eurjchem-29 69 44     SPACE eurjchem-29 69 45 9.76 9.76 NUM eurjchem-29 69 46     SPACE eurjchem-29 69 47 ( ( PUNCT eurjchem-29 69 48 s s PROPN eurjchem-29 69 49 , , PUNCT eurjchem-29 69 50     SPACE eurjchem-29 69 51 1h 1h NUM eurjchem-29 69 52 , , PUNCT eurjchem-29 69 53     SPACE eurjchem-29 69 54 nh nh PROPN eurjchem-29 69 55 ) ) PUNCT eurjchem-29 69 56 . . PUNCT eurjchem-29 69 57     SPACE eurjchem-29 70 1 anal anal ADJ eurjchem-29 70 2 . . PUNCT eurjchem-29 70 3     SPACE eurjchem-29 70 4 calcd calcd NOUN eurjchem-29 70 5 . . PUNCT eurjchem-29 70 6     SPACE eurjchem-29 70 7 for for ADP eurjchem-29 70 8     SPACE eurjchem-29 70 9 c33h20n9o4scl c33h20n9o4scl PROPN eurjchem-29 70 10     SPACE eurjchem-29 70 11 ( ( PUNCT eurjchem-29 70 12 673.5 673.5 NUM eurjchem-29 70 13 ): ): PUNCT eurjchem-29 70 14     SPACE eurjchem-29 70 15 c c NOUN eurjchem-29 70 16 , , PUNCT eurjchem-29 70 17     SPACE eurjchem-29 70 18 58.79 58.79 NUM eurjchem-29 70 19 ; ; PUNCT eurjchem-29 70 20     SPACE eurjchem-29 70 21 h h NOUN eurjchem-29 70 22 , , PUNCT eurjchem-29 70 23     SPACE eurjchem-29 70 24 2.96 2.96 NUM eurjchem-29 70 25 ; ; PUNCT eurjchem-29 70 26     SPACE eurjchem-29 70 27 n n CCONJ eurjchem-29 70 28 , , PUNCT eurjchem-29 70 29     SPACE eurjchem-29 70 30 18.70 18.70 NUM eurjchem-29 70 31 ; ; PUNCT eurjchem-29 70 32     SPACE eurjchem-29 70 33 s s PROPN eurjchem-29 70 34 , , PUNCT eurjchem-29 70 35     SPACE eurjchem-29 70 36 4.75 4.75 NUM eurjchem-29 70 37 ; ; PUNCT eurjchem-29 70 38     SPACE eurjchem-29 70 39 cl cl NOUN eurjchem-29 70 40 , , PUNCT eurjchem-29 70 41     SPACE eurjchem-29 70 42 5.27 5.27 NUM eurjchem-29 70 43 . . PUNCT eurjchem-29 70 44     SPACE eurjchem-29 70 45 found find VERB eurjchem-29 70 46 : : PUNCT eurjchem-29 70 47     SPACE eurjchem-29 70 48 c c X eurjchem-29 70 49 , , PUNCT eurjchem-29 70 50     SPACE eurjchem-29 70 51 58.45 58.45 NUM eurjchem-29 70 52 ; ; PUNCT eurjchem-29 70 53     SPACE eurjchem-29 70 54 h h NOUN eurjchem-29 70 55 , , PUNCT eurjchem-29 70 56     SPACE eurjchem-29 70 57 2.60 2.60 NUM eurjchem-29 70 58 ; ; PUNCT eurjchem-29 70 59     SPACE eurjchem-29 70 60 n n CCONJ eurjchem-29 70 61 , , PUNCT eurjchem-29 70 62     SPACE eurjchem-29 70 63 18.41 18.41 NUM eurjchem-29 70 64 ; ; PUNCT eurjchem-29 70 65     SPACE eurjchem-29 70 66 s s PROPN eurjchem-29 70 67 , , PUNCT eurjchem-29 70 68     SPACE eurjchem-29 70 69 4.46 4.46 NUM eurjchem-29 70 70 ; ; PUNCT eurjchem-29 70 71     SPACE eurjchem-29 70 72 cl cl NOUN eurjchem-29 70 73 , , PUNCT eurjchem-29 70 74     SPACE eurjchem-29 70 75 5.03 5.03 NUM eurjchem-29 70 76     SPACE eurjchem-29 70 77 % % NOUN eurjchem-29 70 78 . . PUNCT eurjchem-29 70 79           SPACE eurjchem-29 70 80 2.2.6 2.2.6 NUM eurjchem-29 70 81 . . PUNCT eurjchem-29 70 82     SPACE eurjchem-29 71 1 8­[5,6­diphenyl­4­(1,3­thiazol­2­yl)­1h­1,2,4­triazin­3­ 8­[5,6­diphenyl­4­(1,3­thiazol­2­yl)­1h­1,2,4­triazin­3­ PROPN eurjchem-29 71 2 yl]­7­(3­nitrophenyl)­5­oxo­1­(2­amino­4h­imidazol­5­ yl]­7­(3­nitrophenyl)­5­oxo­1­(2­amino­4h­imidazol­5­ PROPN eurjchem-29 71 3 yl)[1,2,4]triazolo[1,5­a]pyridine­6­carbonitrile yl)[1,2,4]triazolo[1,5­a]pyridine­6­carbonitrile NOUN eurjchem-29 71 4     SPACE eurjchem-29 71 5 ( ( PUNCT eurjchem-29 71 6 8) 8) NUM eurjchem-29 71 7         SPACE eurjchem-29 71 8 a a DET eurjchem-29 71 9     SPACE eurjchem-29 71 10 mixture mixture NOUN eurjchem-29 71 11     SPACE eurjchem-29 71 12 of of ADP eurjchem-29 71 13     SPACE eurjchem-29 71 14 7 7 NUM eurjchem-29 71 15     SPACE eurjchem-29 71 16 ( ( PUNCT eurjchem-29 71 17 0.01 0.01 NUM eurjchem-29 71 18     SPACE eurjchem-29 71 19 mol mol NOUN eurjchem-29 71 20 ) ) PUNCT eurjchem-29 71 21     SPACE eurjchem-29 71 22 and and CCONJ eurjchem-29 71 23     SPACE eurjchem-29 71 24 guanidine guanidine NOUN eurjchem-29 71 25     SPACE eurjchem-29 71 26 hydrochloride hydrochloride NOUN eurjchem-29 71 27     SPACE eurjchem-29 71 28 ( ( PUNCT eurjchem-29 71 29 0.01 0.01 NUM eurjchem-29 71 30     SPACE eurjchem-29 71 31 mol mol NOUN eurjchem-29 71 32 ) ) PUNCT eurjchem-29 71 33 , , PUNCT eurjchem-29 71 34     SPACE eurjchem-29 71 35 dissolved dissolve VERB eurjchem-29 71 36     SPACE eurjchem-29 71 37 in in ADP eurjchem-29 71 38     SPACE eurjchem-29 71 39 a a DET eurjchem-29 71 40     SPACE eurjchem-29 71 41 little little ADJ eurjchem-29 71 42     SPACE eurjchem-29 71 43 amount amount NOUN eurjchem-29 71 44     SPACE eurjchem-29 71 45 of of ADP eurjchem-29 71 46     SPACE eurjchem-29 71 47 water water NOUN eurjchem-29 71 48     SPACE eurjchem-29 71 49 ( ( PUNCT eurjchem-29 71 50 3 3 NUM eurjchem-29 71 51     SPACE eurjchem-29 71 52 cm3 cm3 NOUN eurjchem-29 71 53 ) ) PUNCT eurjchem-29 71 54 , , PUNCT eurjchem-29 71 55     SPACE eurjchem-29 71 56 in in ADP eurjchem-29 71 57     SPACE eurjchem-29 71 58 dmf dmf PROPN eurjchem-29 71 59     SPACE eurjchem-29 71 60 ( ( PUNCT eurjchem-29 71 61 30 30 NUM eurjchem-29 71 62     SPACE eurjchem-29 71 63 cm3 cm3 NOUN eurjchem-29 71 64 ) ) PUNCT eurjchem-29 71 65     SPACE eurjchem-29 71 66 was be AUX eurjchem-29 71 67     SPACE eurjchem-29 71 68 heated heated ADJ eurjchem-29 71 69     SPACE eurjchem-29 71 70 under under ADP eurjchem-29 71 71     SPACE eurjchem-29 71 72 reflux reflux NOUN eurjchem-29 71 73     SPACE eurjchem-29 71 74 for for ADP eurjchem-29 71 75     SPACE eurjchem-29 71 76 10 10 NUM eurjchem-29 71 77     SPACE eurjchem-29 71 78 h h NOUN eurjchem-29 71 79 , , PUNCT eurjchem-29 71 80     SPACE eurjchem-29 71 81 and and CCONJ eurjchem-29 71 82     SPACE eurjchem-29 71 83 then then ADV eurjchem-29 71 84     SPACE eurjchem-29 71 85 allowed allow VERB eurjchem-29 71 86     SPACE eurjchem-29 71 87 to to PART eurjchem-29 71 88     SPACE eurjchem-29 71 89 cool cool ADJ eurjchem-29 71 90 . . PUNCT eurjchem-29 71 91     SPACE eurjchem-29 72 1 the the DET eurjchem-29 72 2     SPACE eurjchem-29 72 3 reaction reaction NOUN eurjchem-29 72 4     SPACE eurjchem-29 72 5 mixture mixture NOUN eurjchem-29 72 6     SPACE eurjchem-29 72 7 was be AUX eurjchem-29 72 8     SPACE eurjchem-29 72 9 poured pour VERB eurjchem-29 72 10     SPACE eurjchem-29 72 11 onto onto ADP eurjchem-29 72 12     SPACE eurjchem-29 72 13 ice ice NOUN eurjchem-29 72 14     SPACE eurjchem-29 72 15 water water NOUN eurjchem-29 72 16 . . PUNCT eurjchem-29 72 17     SPACE eurjchem-29 73 1 the the DET eurjchem-29 73 2     SPACE eurjchem-29 73 3 solid solid X eurjchem-29 73 4       SPACE eurjchem-29 73 5 170 170 NUM eurjchem-29 73 6     SPACE eurjchem-29 73 7 abdel­monem abdel­monem NOUN eurjchem-29 73 8     SPACE eurjchem-29 73 9 / / SYM eurjchem-29 73 10     SPACE eurjchem-29 73 11 european european ADJ eurjchem-29 73 12     SPACE eurjchem-29 73 13 journal journal NOUN eurjchem-29 73 14     SPACE eurjchem-29 73 15 of of ADP eurjchem-29 73 16     SPACE eurjchem-29 73 17 chemistry chemistry NOUN eurjchem-29 73 18     SPACE eurjchem-29 73 19 1 1 NUM eurjchem-29 73 20     SPACE eurjchem-29 73 21 ( ( PUNCT eurjchem-29 73 22 3 3 NUM eurjchem-29 73 23 ) ) PUNCT eurjchem-29 73 24     SPACE eurjchem-29 73 25 ( ( PUNCT eurjchem-29 73 26 2010 2010 NUM eurjchem-29 73 27 ) ) PUNCT eurjchem-29 73 28     SPACE eurjchem-29 73 29 168­172 168­172 NUM eurjchem-29 73 30             SPACE eurjchem-29 73 31 6a 6a NOUN eurjchem-29 73 32 , , PUNCT eurjchem-29 73 33 b b PROPN eurjchem-29 73 34 1:1 1:1 NUM eurjchem-29 73 35 o o NOUN eurjchem-29 73 36 n n CCONJ eurjchem-29 73 37 hn hn PROPN eurjchem-29 73 38 n n CCONJ eurjchem-29 73 39 - - PUNCT eurjchem-29 73 40 r r NOUN eurjchem-29 73 41 ar ar NOUN eurjchem-29 73 42 ph ph ADJ eurjchem-29 73 43 ph ph PROPN eurjchem-29 73 44 n n CCONJ eurjchem-29 73 45 n n CCONJ eurjchem-29 73 46 n n NOUN eurjchem-29 73 47 o o PROPN eurjchem-29 73 48 cl cl NOUN eurjchem-29 73 49 nc nc PROPN eurjchem-29 73 50 7 7 NUM eurjchem-29 73 51 nh2 nh2 PROPN eurjchem-29 73 52 nc nc PROPN eurjchem-29 73 53 n n PROPN eurjchem-29 73 54 n n CCONJ eurjchem-29 73 55 n n ADV eurjchem-29 73 56 nh2 nh2 PROPN eurjchem-29 73 57 o o PROPN eurjchem-29 73 58 n n CCONJ eurjchem-29 73 59 hn hn PROPN eurjchem-29 73 60 n n CCONJ eurjchem-29 73 61 - - PUNCT eurjchem-29 73 62 r r NOUN eurjchem-29 73 63 ar ar NOUN eurjchem-29 73 64 ph ph ADJ eurjchem-29 73 65 ph ph PROPN eurjchem-29 73 66 n n CCONJ eurjchem-29 73 67 n n ADV eurjchem-29 73 68 8 8 NUM eurjchem-29 73 69 o o NOUN eurjchem-29 73 70 n n CCONJ eurjchem-29 73 71 hn hn PROPN eurjchem-29 73 72 n n CCONJ eurjchem-29 73 73 - - PUNCT eurjchem-29 73 74 r r NOUN eurjchem-29 73 75 ar ar NOUN eurjchem-29 73 76 ph ph ADJ eurjchem-29 73 77 ph ph PROPN eurjchem-29 73 78 n n CCONJ eurjchem-29 73 79 n n CCONJ eurjchem-29 73 80 n n CCONJ eurjchem-29 73 81 n n CCONJ eurjchem-29 73 82 n n PROPN eurjchem-29 73 83 nh nh PROPN eurjchem-29 73 84 ch3 ch3 PROPN eurjchem-29 73 85 o o PROPN eurjchem-29 73 86 nc nc PROPN eurjchem-29 73 87 ar ar PROPN eurjchem-29 73 88 o o PROPN eurjchem-29 73 89 n n CCONJ eurjchem-29 73 90 hn hn PROPN eurjchem-29 73 91 n n CCONJ eurjchem-29 73 92 - - PUNCT eurjchem-29 73 93 r r NOUN eurjchem-29 73 94 ph ph NOUN eurjchem-29 73 95 ph ph NOUN eurjchem-29 73 96 cn cn PROPN eurjchem-29 73 97 n n CCONJ eurjchem-29 73 98 n n CCONJ eurjchem-29 73 99 n n CCONJ eurjchem-29 73 100 o o NOUN eurjchem-29 73 101 oet oet ADJ eurjchem-29 73 102 n n PRON eurjchem-29 73 103 conhnh2 conhnh2 NOUN eurjchem-29 73 104 ar ar NOUN eurjchem-29 73 105 o o PROPN eurjchem-29 73 106 n n CCONJ eurjchem-29 73 107 hn hn PROPN eurjchem-29 73 108 n n CCONJ eurjchem-29 73 109 - - PUNCT eurjchem-29 73 110 r r NOUN eurjchem-29 73 111 ph ph NOUN eurjchem-29 73 112 ph ph NOUN eurjchem-29 73 113 cn cn PROPN eurjchem-29 73 114 n n PROPN eurjchem-29 73 115 n n PROPN eurjchem-29 73 116 ar ar NOUN eurjchem-29 73 117 o o PROPN eurjchem-29 73 118 n n CCONJ eurjchem-29 73 119 hn hn PROPN eurjchem-29 73 120 n n CCONJ eurjchem-29 73 121 - - PUNCT eurjchem-29 73 122 r r NOUN eurjchem-29 73 123 ph ph NOUN eurjchem-29 73 124 ph ph NOUN eurjchem-29 73 125 cn cn PROPN eurjchem-29 73 126 n n CCONJ eurjchem-29 73 127 n n PROPN eurjchem-29 73 128 n n PROPN eurjchem-29 73 129 conhnhcsnh2 conhnhcsnh2 PROPN eurjchem-29 73 130 ar ar NOUN eurjchem-29 73 131 o o PROPN eurjchem-29 73 132 n n CCONJ eurjchem-29 73 133 hn hn PROPN eurjchem-29 73 134 n n CCONJ eurjchem-29 73 135 - - PUNCT eurjchem-29 73 136 r r NOUN eurjchem-29 73 137 ph ph NOUN eurjchem-29 73 138 ph ph NOUN eurjchem-29 73 139 cn cn PROPN eurjchem-29 73 140 n n CCONJ eurjchem-29 73 141 n n CCONJ eurjchem-29 73 142 n n CCONJ eurjchem-29 73 143 n n PROPN eurjchem-29 73 144 h h NOUN eurjchem-29 73 145 nh nh PROPN eurjchem-29 73 146 n n PROPN eurjchem-29 73 147 s s PART eurjchem-29 73 148 13 13 NUM eurjchem-29 73 149 12 12 NUM eurjchem-29 73 150 etoh+hcl etoh+hcl VERB eurjchem-29 73 151 11 11 NUM eurjchem-29 73 152 10 10 NUM eurjchem-29 73 153 r= r= ADJ eurjchem-29 73 154 n n PROPN eurjchem-29 73 155 s s PART eurjchem-29 73 156 acoh/ acoh/ NUM eurjchem-29 73 157 6b6a 6b6a NOUN eurjchem-29 73 158 1:1 1:1 NUM eurjchem-29 73 159 acoh/ acoh/ NUM eurjchem-29 73 160 9 9 NUM eurjchem-29 73 161 a a PRON eurjchem-29 73 162 , , PUNCT eurjchem-29 73 163 ar= ar= ADJ eurjchem-29 73 164 4 4 NUM eurjchem-29 73 165 - - NOUN eurjchem-29 73 166 clc6h4 clc6h4 NOUN eurjchem-29 73 167 b b NOUN eurjchem-29 73 168 , , PUNCT eurjchem-29 73 169 ar= ar= ADJ eurjchem-29 73 170 3 3 NUM eurjchem-29 73 171 - - PUNCT eurjchem-29 73 172 no2c6h4 no2c6h4 PROPN eurjchem-29 73 173 clch2cocl clch2cocl NOUN eurjchem-29 73 174 dmf dmf PROPN eurjchem-29 73 175 dmf dmf PROPN eurjchem-29 73 176 h2n h2n PROPN eurjchem-29 73 177 nh nh PROPN eurjchem-29 73 178 clch2cooet clch2cooet PROPN eurjchem-29 73 179 dmf dmf PROPN eurjchem-29 73 180 nh4ncs nh4ncs PROPN eurjchem-29 73 181 etoh etoh PROPN eurjchem-29 73 182 n2h4.h2o n2h4.h2o NOUN eurjchem-29 73 183 naoac naoac NOUN eurjchem-29 73 184 naoac naoac VERB eurjchem-29 73 185     SPACE eurjchem-29 73 186 scheme scheme NOUN eurjchem-29 73 187     SPACE eurjchem-29 73 188 2 2 NUM eurjchem-29 73 189             SPACE eurjchem-29 73 190 product product NOUN eurjchem-29 73 191     SPACE eurjchem-29 73 192 that that PRON eurjchem-29 73 193     SPACE eurjchem-29 73 194 formed form VERB eurjchem-29 73 195     SPACE eurjchem-29 73 196 was be AUX eurjchem-29 73 197     SPACE eurjchem-29 73 198 filtered filter VERB eurjchem-29 73 199     SPACE eurjchem-29 73 200 off off ADP eurjchem-29 73 201 , , PUNCT eurjchem-29 73 202     SPACE eurjchem-29 73 203 dried dry VERB eurjchem-29 73 204     SPACE eurjchem-29 73 205 and and CCONJ eurjchem-29 73 206     SPACE eurjchem-29 73 207 crystallized crystallize VERB eurjchem-29 73 208     SPACE eurjchem-29 73 209 from from ADP eurjchem-29 73 210     SPACE eurjchem-29 73 211 methanol methanol NOUN eurjchem-29 73 212     SPACE eurjchem-29 73 213 ( ( PUNCT eurjchem-29 73 214 scheme scheme NOUN eurjchem-29 73 215     SPACE eurjchem-29 73 216 2 2 NUM eurjchem-29 73 217 ) ) PUNCT eurjchem-29 73 218 . . PUNCT eurjchem-29 73 219     SPACE eurjchem-29 74 1 yield yield NOUN eurjchem-29 74 2 : : PUNCT eurjchem-29 74 3     SPACE eurjchem-29 74 4 60 60 NUM eurjchem-29 74 5 % % NOUN eurjchem-29 74 6 . . PUNCT eurjchem-29 74 7     SPACE eurjchem-29 75 1 m.p m.p PROPN eurjchem-29 75 2 . . PROPN eurjchem-29 75 3 : : PUNCT eurjchem-29 75 4     SPACE eurjchem-29 75 5 227‐ 227‐ NUM eurjchem-29 75 6     SPACE eurjchem-29 75 7 230 230 NUM eurjchem-29 75 8     SPACE eurjchem-29 75 9 ° ° NOUN eurjchem-29 75 10 c c NOUN eurjchem-29 75 11 . . PUNCT eurjchem-29 75 12     SPACE eurjchem-29 76 1 ft‐ ft‐ PROPN eurjchem-29 76 2     SPACE eurjchem-29 76 3 ir ir PROPN eurjchem-29 76 4     SPACE eurjchem-29 76 5 ( ( PUNCT eurjchem-29 76 6 kbr kbr PROPN eurjchem-29 76 7 ) ) PUNCT eurjchem-29 76 8     SPACE eurjchem-29 76 9 ν ν NOUN eurjchem-29 76 10 , , PUNCT eurjchem-29 76 11     SPACE eurjchem-29 76 12 ( ( PUNCT eurjchem-29 76 13 cm‐1 cm‐1 NOUN eurjchem-29 76 14 ): ): PUNCT eurjchem-29 76 15     SPACE eurjchem-29 76 16 3395 3395 NUM eurjchem-29 76 17 , , PUNCT eurjchem-29 76 18     SPACE eurjchem-29 76 19 2930(nh2 2930(nh2 NUM eurjchem-29 76 20 ) ) PUNCT eurjchem-29 76 21 , , PUNCT eurjchem-29 76 22     SPACE eurjchem-29 76 23 1487 1487 NUM eurjchem-29 76 24     SPACE eurjchem-29 76 25 ( ( PUNCT eurjchem-29 76 26 def def ADJ eurjchem-29 76 27 . . PUNCT eurjchem-29 76 28     SPACE eurjchem-29 76 29 ch2 ch2 PROPN eurjchem-29 76 30 ) ) PUNCT eurjchem-29 76 31 , , PUNCT eurjchem-29 76 32     SPACE eurjchem-29 76 33 2213 2213 NUM eurjchem-29 76 34     SPACE eurjchem-29 76 35 ( ( PUNCT eurjchem-29 76 36 c≡n c≡n PROPN eurjchem-29 76 37 ) ) PUNCT eurjchem-29 76 38 , , PUNCT eurjchem-29 76 39     SPACE eurjchem-29 76 40 1686 1686 NUM eurjchem-29 76 41     SPACE eurjchem-29 76 42 ( ( PUNCT eurjchem-29 76 43 c c NOUN eurjchem-29 76 44 = = NOUN eurjchem-29 76 45 o o NOUN eurjchem-29 76 46 ) ) PUNCT eurjchem-29 76 47 , , PUNCT eurjchem-29 76 48     SPACE eurjchem-29 76 49 1578 1578 NUM eurjchem-29 76 50     SPACE eurjchem-29 76 51 ( ( PUNCT eurjchem-29 76 52 c c NOUN eurjchem-29 76 53 = = SYM eurjchem-29 76 54 n n NUM eurjchem-29 76 55 ) ) PUNCT eurjchem-29 76 56 . . PUNCT eurjchem-29 76 57     SPACE eurjchem-29 77 1 1h 1h NUM eurjchem-29 77 2     SPACE eurjchem-29 77 3 nmr nmr NOUN eurjchem-29 77 4     SPACE eurjchem-29 77 5 ( ( PUNCT eurjchem-29 77 6 200 200 NUM eurjchem-29 77 7     SPACE eurjchem-29 77 8 mhz mhz NOUN eurjchem-29 77 9 , , PUNCT eurjchem-29 77 10     SPACE eurjchem-29 77 11 dmso‐d6 dmso‐d6 NOUN eurjchem-29 77 12 ) ) PUNCT eurjchem-29 77 13 , , PUNCT eurjchem-29 77 14     SPACE eurjchem-29 77 15 δ δ PROPN eurjchem-29 77 16 : : PUNCT eurjchem-29 77 17     SPACE eurjchem-29 77 18 6.55 6.55 NUM eurjchem-29 77 19     SPACE eurjchem-29 77 20 ( ( PUNCT eurjchem-29 77 21 s s PROPN eurjchem-29 77 22 , , PUNCT eurjchem-29 77 23     SPACE eurjchem-29 77 24 br br PROPN eurjchem-29 77 25 , , PUNCT eurjchem-29 77 26     SPACE eurjchem-29 77 27 2h 2h NUM eurjchem-29 77 28 , , PUNCT eurjchem-29 77 29     SPACE eurjchem-29 77 30 nh2 nh2 PROPN eurjchem-29 77 31 ) ) PUNCT eurjchem-29 77 32 , , PUNCT eurjchem-29 77 33     SPACE eurjchem-29 77 34 7.64–8.53 7.64–8.53 NUM eurjchem-29 77 35     SPACE eurjchem-29 77 36 ( ( PUNCT eurjchem-29 77 37 m m PROPN eurjchem-29 77 38 , , PUNCT eurjchem-29 77 39     SPACE eurjchem-29 77 40 20h 20h NOUN eurjchem-29 77 41 , , PUNCT eurjchem-29 77 42     SPACE eurjchem-29 77 43 ar‐h ar‐h NOUN eurjchem-29 77 44 ) ) PUNCT eurjchem-29 77 45 , , PUNCT eurjchem-29 77 46     SPACE eurjchem-29 77 47 8.98 8.98 NUM eurjchem-29 77 48     SPACE eurjchem-29 77 49 ( ( PUNCT eurjchem-29 77 50 s s PROPN eurjchem-29 77 51 , , PUNCT eurjchem-29 77 52     SPACE eurjchem-29 77 53 1h 1h NUM eurjchem-29 77 54 , , PUNCT eurjchem-29 77 55     SPACE eurjchem-29 77 56 nh nh PROPN eurjchem-29 77 57 ) ) PUNCT eurjchem-29 77 58 . . PUNCT eurjchem-29 77 59     SPACE eurjchem-29 78 1 ms ms PROPN eurjchem-29 78 2 , , PUNCT eurjchem-29 78 3     SPACE eurjchem-29 78 4 m m PROPN eurjchem-29 78 5 / / PROPN eurjchem-29 78 6 z z NOUN eurjchem-29 78 7     SPACE eurjchem-29 78 8 ( ( PUNCT eurjchem-29 78 9 i i PRON eurjchem-29 78 10     SPACE eurjchem-29 78 11 % % VERB eurjchem-29 78 12 ): ): PUNCT eurjchem-29 78 13     SPACE eurjchem-29 78 14 677 677 NUM eurjchem-29 78 15     SPACE eurjchem-29 78 16 ( ( PUNCT eurjchem-29 78 17 m+ m+ NUM eurjchem-29 78 18 , , PUNCT eurjchem-29 78 19     SPACE eurjchem-29 78 20 10 10 NUM eurjchem-29 78 21 % % NOUN eurjchem-29 78 22 ) ) PUNCT eurjchem-29 78 23 , , PUNCT eurjchem-29 78 24     SPACE eurjchem-29 78 25 597 597 NUM eurjchem-29 78 26     SPACE eurjchem-29 78 27 ( ( PUNCT eurjchem-29 78 28 11 11 NUM eurjchem-29 78 29 ) ) PUNCT eurjchem-29 78 30 , , PUNCT eurjchem-29 78 31     SPACE eurjchem-29 78 32 421 421 NUM eurjchem-29 78 33     SPACE eurjchem-29 78 34 ( ( PUNCT eurjchem-29 78 35 13 13 NUM eurjchem-29 78 36 ) ) PUNCT eurjchem-29 78 37 , , PUNCT eurjchem-29 78 38     SPACE eurjchem-29 78 39 317 317 NUM eurjchem-29 78 40     SPACE eurjchem-29 78 41 ( ( PUNCT eurjchem-29 78 42 100 100 NUM eurjchem-29 78 43 ) ) PUNCT eurjchem-29 78 44 , , PUNCT eurjchem-29 78 45     SPACE eurjchem-29 78 46 227 227 NUM eurjchem-29 78 47     SPACE eurjchem-29 78 48 ( ( PUNCT eurjchem-29 78 49 3 3 NUM eurjchem-29 78 50 ) ) PUNCT eurjchem-29 78 51 , , PUNCT eurjchem-29 78 52     SPACE eurjchem-29 78 53 216 216 NUM eurjchem-29 78 54     SPACE eurjchem-29 78 55 ( ( PUNCT eurjchem-29 78 56 6 6 NUM eurjchem-29 78 57 ) ) PUNCT eurjchem-29 78 58 , , PUNCT eurjchem-29 78 59     SPACE eurjchem-29 78 60 115 115 NUM eurjchem-29 78 61     SPACE eurjchem-29 78 62 ( ( PUNCT eurjchem-29 78 63 21 21 NUM eurjchem-29 78 64 ) ) PUNCT eurjchem-29 78 65 , , PUNCT eurjchem-29 78 66     SPACE eurjchem-29 78 67 57 57 NUM eurjchem-29 78 68     SPACE eurjchem-29 78 69 ( ( PUNCT eurjchem-29 78 70 11 11 NUM eurjchem-29 78 71 ) ) PUNCT eurjchem-29 78 72 . . PUNCT eurjchem-29 78 73     SPACE eurjchem-29 79 1 anal anal ADJ eurjchem-29 79 2 . . PUNCT eurjchem-29 79 3     SPACE eurjchem-29 79 4 calcd calcd NOUN eurjchem-29 79 5 . . PUNCT eurjchem-29 79 6     SPACE eurjchem-29 79 7 for for ADP eurjchem-29 79 8     SPACE eurjchem-29 79 9 c34h21n12o3s c34h21n12o3s NOUN eurjchem-29 79 10     SPACE eurjchem-29 79 11 ( ( PUNCT eurjchem-29 79 12 677 677 NUM eurjchem-29 79 13 ): ): PUNCT eurjchem-29 79 14     SPACE eurjchem-29 79 15 c c NOUN eurjchem-29 79 16 , , PUNCT eurjchem-29 79 17     SPACE eurjchem-29 79 18 60.26 60.26 NUM eurjchem-29 79 19 ; ; PUNCT eurjchem-29 79 20     SPACE eurjchem-29 79 21 h h NOUN eurjchem-29 79 22 , , PUNCT eurjchem-29 79 23     SPACE eurjchem-29 79 24 3.21 3.21 NUM eurjchem-29 79 25 ; ; PUNCT eurjchem-29 79 26     SPACE eurjchem-29 79 27 n n CCONJ eurjchem-29 79 28 , , PUNCT eurjchem-29 79 29     SPACE eurjchem-29 79 30 24.81 24.81 NUM eurjchem-29 79 31 ; ; PUNCT eurjchem-29 79 32     SPACE eurjchem-29 79 33 s s PROPN eurjchem-29 79 34 , , PUNCT eurjchem-29 79 35     SPACE eurjchem-29 79 36 4.72 4.72 NUM eurjchem-29 79 37 . . PUNCT eurjchem-29 79 38     SPACE eurjchem-29 79 39 found find VERB eurjchem-29 79 40 : : PUNCT eurjchem-29 79 41     SPACE eurjchem-29 79 42 c c X eurjchem-29 79 43 , , PUNCT eurjchem-29 79 44     SPACE eurjchem-29 79 45 59.93 59.93 NUM eurjchem-29 79 46 ; ; PUNCT eurjchem-29 79 47     SPACE eurjchem-29 79 48 h h NOUN eurjchem-29 79 49 , , PUNCT eurjchem-29 79 50     SPACE eurjchem-29 79 51 3.43 3.43 NUM eurjchem-29 79 52 ; ; PUNCT eurjchem-29 79 53     SPACE eurjchem-29 79 54 n n CCONJ eurjchem-29 79 55 , , PUNCT eurjchem-29 79 56     SPACE eurjchem-29 79 57 24.45 24.45 NUM eurjchem-29 79 58 ; ; PUNCT eurjchem-29 79 59     SPACE eurjchem-29 79 60 s s PROPN eurjchem-29 79 61 , , PUNCT eurjchem-29 79 62     SPACE eurjchem-29 79 63 4.37 4.37 NUM eurjchem-29 79 64 % % NOUN eurjchem-29 79 65 . . PUNCT eurjchem-29 79 66           SPACE eurjchem-29 80 1 2.2.7 2.2.7 X eurjchem-29 80 2 . . PUNCT eurjchem-29 80 3     SPACE eurjchem-29 81 1 8­[5,6­diphenyl­4­(1,3­thiazol­2­yl)­1h­1,2,4­triazin­3­ 8­[5,6­diphenyl­4­(1,3­thiazol­2­yl)­1h­1,2,4­triazin­3­ PROPN eurjchem-29 81 2 yl]3­[6­cyano­7­(3­nitro­phenyl­5­oxo­[1,2,4]triazolo[1,5­ yl]3­[6­cyano­7­(3­nitro­phenyl­5­oxo­[1,2,4]triazolo[1,5­ PROPN eurjchem-29 81 3 a]pyridine­8­yl]­1­(4h­imidazol­2­yl)acetamide a]pyridine­8­yl]­1­(4h­imidazol­2­yl)acetamide PROPN eurjchem-29 81 4     SPACE eurjchem-29 81 5 ( ( PUNCT eurjchem-29 81 6 9 9 NUM eurjchem-29 81 7 ) ) PUNCT eurjchem-29 81 8         SPACE eurjchem-29 81 9 a a DET eurjchem-29 81 10     SPACE eurjchem-29 81 11 suspension suspension NOUN eurjchem-29 81 12     SPACE eurjchem-29 81 13 of of ADP eurjchem-29 81 14     SPACE eurjchem-29 81 15 8 8 NUM eurjchem-29 81 16     SPACE eurjchem-29 81 17 ( ( PUNCT eurjchem-29 81 18 0.01 0.01 NUM eurjchem-29 81 19     SPACE eurjchem-29 81 20 mol mol NOUN eurjchem-29 81 21 ) ) PUNCT eurjchem-29 81 22     SPACE eurjchem-29 81 23 in in ADP eurjchem-29 81 24     SPACE eurjchem-29 81 25 glacial glacial ADJ eurjchem-29 81 26     SPACE eurjchem-29 81 27 acetic acetic ADJ eurjchem-29 81 28     SPACE eurjchem-29 81 29 acid acid NOUN eurjchem-29 81 30     SPACE eurjchem-29 81 31 ( ( PUNCT eurjchem-29 81 32 30 30 NUM eurjchem-29 81 33     SPACE eurjchem-29 81 34 cm3 cm3 NOUN eurjchem-29 81 35 ) ) PUNCT eurjchem-29 81 36     SPACE eurjchem-29 81 37 with with ADP eurjchem-29 81 38     SPACE eurjchem-29 81 39 fused fuse VERB eurjchem-29 81 40     SPACE eurjchem-29 81 41 sodium sodium NOUN eurjchem-29 81 42     SPACE eurjchem-29 81 43 acetate acetate NOUN eurjchem-29 81 44     SPACE eurjchem-29 81 45 ( ( PUNCT eurjchem-29 81 46 3 3 NUM eurjchem-29 81 47     SPACE eurjchem-29 81 48 g g NOUN eurjchem-29 81 49 ) ) PUNCT eurjchem-29 81 50     SPACE eurjchem-29 81 51 was be AUX eurjchem-29 81 52     SPACE eurjchem-29 81 53 heated heated ADJ eurjchem-29 81 54     SPACE eurjchem-29 81 55 under under ADP eurjchem-29 81 56     SPACE eurjchem-29 81 57 reflux reflux NOUN eurjchem-29 81 58     SPACE eurjchem-29 81 59 for for ADP eurjchem-29 81 60     SPACE eurjchem-29 81 61 4 4 NUM eurjchem-29 81 62     SPACE eurjchem-29 81 63 h h NOUN eurjchem-29 81 64     SPACE eurjchem-29 81 65 , , PUNCT eurjchem-29 81 66     SPACE eurjchem-29 81 67 cooled cool VERB eurjchem-29 81 68     SPACE eurjchem-29 81 69 and and CCONJ eurjchem-29 81 70     SPACE eurjchem-29 81 71 poured pour VERB eurjchem-29 81 72     SPACE eurjchem-29 81 73 onto onto ADP eurjchem-29 81 74     SPACE eurjchem-29 81 75 crushed crushed ADJ eurjchem-29 81 76     SPACE eurjchem-29 81 77 ice ice NOUN eurjchem-29 81 78 . . PUNCT eurjchem-29 81 79     SPACE eurjchem-29 82 1 the the DET eurjchem-29 82 2     SPACE eurjchem-29 82 3 precipitate precipitate NOUN eurjchem-29 82 4     SPACE eurjchem-29 82 5 that that PRON eurjchem-29 82 6     SPACE eurjchem-29 82 7 formed form VERB eurjchem-29 82 8     SPACE eurjchem-29 82 9 was be AUX eurjchem-29 82 10     SPACE eurjchem-29 82 11 filtered filter VERB eurjchem-29 82 12     SPACE eurjchem-29 82 13 off off ADP eurjchem-29 82 14 , , PUNCT eurjchem-29 82 15     SPACE eurjchem-29 82 16 dried dry VERB eurjchem-29 82 17     SPACE eurjchem-29 82 18 and and CCONJ eurjchem-29 82 19     SPACE eurjchem-29 82 20 crystallized crystallize VERB eurjchem-29 82 21     SPACE eurjchem-29 82 22 from from ADP eurjchem-29 82 23     SPACE eurjchem-29 82 24 benzene benzene NOUN eurjchem-29 82 25     SPACE eurjchem-29 82 26 ( ( PUNCT eurjchem-29 82 27 scheme scheme NOUN eurjchem-29 82 28     SPACE eurjchem-29 82 29 2 2 NUM eurjchem-29 82 30 ) ) PUNCT eurjchem-29 82 31 . . PUNCT eurjchem-29 82 32     SPACE eurjchem-29 82 33 yield yield NOUN eurjchem-29 82 34 : : PUNCT eurjchem-29 82 35     SPACE eurjchem-29 82 36 59 59 NUM eurjchem-29 82 37 % % NOUN eurjchem-29 82 38 . . PUNCT eurjchem-29 82 39     SPACE eurjchem-29 83 1 m.p m.p PROPN eurjchem-29 83 2 . . PROPN eurjchem-29 83 3 : : PUNCT eurjchem-29 83 4     SPACE eurjchem-29 84 1 221‐223 221‐223 NOUN eurjchem-29 84 2     SPACE eurjchem-29 84 3 ° ° PROPN eurjchem-29 84 4 c c NOUN eurjchem-29 84 5 . . PUNCT eurjchem-29 84 6     SPACE eurjchem-29 84 7 ft‐ ft‐ AUX eurjchem-29 84 8     SPACE eurjchem-29 84 9 ir ir VERB eurjchem-29 84 10     SPACE eurjchem-29 84 11 ( ( PUNCT eurjchem-29 84 12 kbr kbr PROPN eurjchem-29 84 13 ) ) PUNCT eurjchem-29 84 14     SPACE eurjchem-29 84 15 ν ν PROPN eurjchem-29 84 16 , , PUNCT eurjchem-29 84 17     SPACE eurjchem-29 84 18 ( ( PUNCT eurjchem-29 84 19 cm‐1 cm‐1 NOUN eurjchem-29 84 20 ): ): PUNCT eurjchem-29 84 21     SPACE eurjchem-29 84 22 3278 3278 NUM eurjchem-29 84 23     SPACE eurjchem-29 84 24 ( ( PUNCT eurjchem-29 84 25 nh nh NOUN eurjchem-29 84 26 ) ) PUNCT eurjchem-29 84 27 , , PUNCT eurjchem-29 84 28     SPACE eurjchem-29 84 29 2982 2982 NUM eurjchem-29 84 30     SPACE eurjchem-29 84 31 ( ( PUNCT eurjchem-29 84 32 ch3 ch3 PROPN eurjchem-29 84 33 ) ) PUNCT eurjchem-29 84 34 , , PUNCT eurjchem-29 84 35     SPACE eurjchem-29 84 36 2845 2845 NUM eurjchem-29 84 37     SPACE eurjchem-29 84 38 ( ( PUNCT eurjchem-29 84 39 ch2 ch2 PROPN eurjchem-29 84 40 ) ) PUNCT eurjchem-29 84 41 , , PUNCT eurjchem-29 84 42     SPACE eurjchem-29 84 43 2217 2217 NUM eurjchem-29 84 44     SPACE eurjchem-29 84 45 ( ( PUNCT eurjchem-29 84 46 c≡n c≡n PROPN eurjchem-29 84 47 ) ) PUNCT eurjchem-29 84 48 , , PUNCT eurjchem-29 84 49     SPACE eurjchem-29 84 50 1676 1676 NUM eurjchem-29 84 51 , , PUNCT eurjchem-29 84 52     SPACE eurjchem-29 84 53 1662 1662 NUM eurjchem-29 84 54     SPACE eurjchem-29 84 55 ( ( PUNCT eurjchem-29 84 56 2 2 NUM eurjchem-29 84 57     SPACE eurjchem-29 84 58 c c NOUN eurjchem-29 84 59 = = NOUN eurjchem-29 84 60 o o NOUN eurjchem-29 84 61 ) ) PUNCT eurjchem-29 84 62 , , PUNCT eurjchem-29 84 63     SPACE eurjchem-29 84 64 1594 1594 NUM eurjchem-29 84 65     SPACE eurjchem-29 84 66 ( ( PUNCT eurjchem-29 84 67 c c NOUN eurjchem-29 84 68 = = SYM eurjchem-29 84 69 n n NUM eurjchem-29 84 70 ) ) PUNCT eurjchem-29 84 71 . . PUNCT eurjchem-29 84 72     SPACE eurjchem-29 85 1 1h 1h NUM eurjchem-29 85 2     SPACE eurjchem-29 85 3 nmr nmr NOUN eurjchem-29 85 4     SPACE eurjchem-29 85 5 ( ( PUNCT eurjchem-29 85 6 200 200 NUM eurjchem-29 85 7     SPACE eurjchem-29 85 8 mhz mhz NOUN eurjchem-29 85 9 , , PUNCT eurjchem-29 85 10     SPACE eurjchem-29 85 11 dmso‐d6 dmso‐d6 NOUN eurjchem-29 85 12 ) ) PUNCT eurjchem-29 85 13 , , PUNCT eurjchem-29 85 14     SPACE eurjchem-29 85 15 δ δ PROPN eurjchem-29 85 16 : : PUNCT eurjchem-29 85 17     SPACE eurjchem-29 85 18 2.68 2.68 NUM eurjchem-29 85 19     SPACE eurjchem-29 85 20 ( ( PUNCT eurjchem-29 85 21 s s PROPN eurjchem-29 85 22 , , PUNCT eurjchem-29 85 23     SPACE eurjchem-29 85 24 3h 3h NUM eurjchem-29 85 25 , , PUNCT eurjchem-29 85 26     SPACE eurjchem-29 85 27 ch3 ch3 PROPN eurjchem-29 85 28 ) ) PUNCT eurjchem-29 85 29 , , PUNCT eurjchem-29 85 30     SPACE eurjchem-29 85 31 7.36–8.28 7.36–8.28 NUM eurjchem-29 85 32 , , PUNCT eurjchem-29 85 33     SPACE eurjchem-29 85 34 ( ( PUNCT eurjchem-29 85 35 m m PROPN eurjchem-29 85 36 , , PUNCT eurjchem-29 85 37     SPACE eurjchem-29 85 38 22h 22h NOUN eurjchem-29 85 39 , , PUNCT eurjchem-29 85 40     SPACE eurjchem-29 85 41 ar‐h ar‐h NOUN eurjchem-29 85 42 ) ) PUNCT eurjchem-29 85 43 , , PUNCT eurjchem-29 85 44     SPACE eurjchem-29 85 45 8.78 8.78 NUM eurjchem-29 85 46     SPACE eurjchem-29 85 47 ( ( PUNCT eurjchem-29 85 48 s s PROPN eurjchem-29 85 49 , , PUNCT eurjchem-29 85 50     SPACE eurjchem-29 85 51 1h 1h NUM eurjchem-29 85 52 , , PUNCT eurjchem-29 85 53     SPACE eurjchem-29 85 54 nh nh PROPN eurjchem-29 85 55 ) ) PUNCT eurjchem-29 85 56 , , PUNCT eurjchem-29 85 57     SPACE eurjchem-29 85 58 9.37 9.37 NUM eurjchem-29 85 59     SPACE eurjchem-29 85 60 ( ( PUNCT eurjchem-29 85 61 s s PROPN eurjchem-29 85 62 , , PUNCT eurjchem-29 85 63     SPACE eurjchem-29 85 64 1h 1h NUM eurjchem-29 85 65 , , PUNCT eurjchem-29 85 66     SPACE eurjchem-29 85 67 nh nh PROPN eurjchem-29 85 68 ) ) PUNCT eurjchem-29 85 69 . . PUNCT eurjchem-29 85 70     SPACE eurjchem-29 86 1 ms ms PROPN eurjchem-29 86 2 , , PUNCT eurjchem-29 86 3     SPACE eurjchem-29 86 4 m m PROPN eurjchem-29 86 5 / / PROPN eurjchem-29 86 6 z z NOUN eurjchem-29 86 7     SPACE eurjchem-29 86 8 ( ( PUNCT eurjchem-29 86 9 i i PRON eurjchem-29 86 10     SPACE eurjchem-29 86 11 % % VERB eurjchem-29 86 12 ): ): PUNCT eurjchem-29 86 13     SPACE eurjchem-29 86 14 719 719 NUM eurjchem-29 86 15     SPACE eurjchem-29 86 16 ( ( PUNCT eurjchem-29 86 17 m+ m+ NUM eurjchem-29 86 18 , , PUNCT eurjchem-29 86 19     SPACE eurjchem-29 86 20 11 11 NUM eurjchem-29 86 21 % % NOUN eurjchem-29 86 22 ) ) PUNCT eurjchem-29 86 23 , , PUNCT eurjchem-29 86 24     SPACE eurjchem-29 86 25 597 597 NUM eurjchem-29 86 26     SPACE eurjchem-29 86 27 ( ( PUNCT eurjchem-29 86 28 19 19 NUM eurjchem-29 86 29 ) ) PUNCT eurjchem-29 86 30 , , PUNCT eurjchem-29 86 31     SPACE eurjchem-29 86 32 443 443 NUM eurjchem-29 86 33     SPACE eurjchem-29 86 34 ( ( PUNCT eurjchem-29 86 35 15 15 NUM eurjchem-29 86 36 ) ) PUNCT eurjchem-29 86 37 , , PUNCT eurjchem-29 86 38     SPACE eurjchem-29 86 39 363 363 NUM eurjchem-29 86 40     SPACE eurjchem-29 86 41 ( ( PUNCT eurjchem-29 86 42 11 11 NUM eurjchem-29 86 43 ) ) PUNCT eurjchem-29 86 44 , , PUNCT eurjchem-29 86 45     SPACE eurjchem-29 86 46 252 252 NUM eurjchem-29 86 47     SPACE eurjchem-29 86 48 ( ( PUNCT eurjchem-29 86 49 31 31 NUM eurjchem-29 86 50 ) ) PUNCT eurjchem-29 86 51 , , PUNCT eurjchem-29 86 52     SPACE eurjchem-29 86 53 216 216 NUM eurjchem-29 86 54     SPACE eurjchem-29 86 55 ( ( PUNCT eurjchem-29 86 56 38 38 NUM eurjchem-29 86 57 ) ) PUNCT eurjchem-29 86 58     SPACE eurjchem-29 86 59 178 178 NUM eurjchem-29 86 60     SPACE eurjchem-29 86 61 ( ( PUNCT eurjchem-29 86 62 63 63 NUM eurjchem-29 86 63 ) ) PUNCT eurjchem-29 86 64 , , PUNCT eurjchem-29 86 65     SPACE eurjchem-29 86 66 158 158 NUM eurjchem-29 86 67     SPACE eurjchem-29 86 68 ( ( PUNCT eurjchem-29 86 69 32 32 NUM eurjchem-29 86 70 ) ) PUNCT eurjchem-29 86 71 , , PUNCT eurjchem-29 86 72     SPACE eurjchem-29 86 73 77 77 NUM eurjchem-29 86 74     SPACE eurjchem-29 86 75 ( ( PUNCT eurjchem-29 86 76 100 100 NUM eurjchem-29 86 77 ) ) PUNCT eurjchem-29 86 78 , , PUNCT eurjchem-29 86 79     SPACE eurjchem-29 86 80 57(21 57(21 NUM eurjchem-29 86 81 ) ) PUNCT eurjchem-29 86 82 . . PUNCT eurjchem-29 86 83     SPACE eurjchem-29 87 1 anal anal ADJ eurjchem-29 87 2 . . PUNCT eurjchem-29 87 3     SPACE eurjchem-29 87 4 calcd calcd NOUN eurjchem-29 87 5 . . PUNCT eurjchem-29 87 6     SPACE eurjchem-29 87 7 for for ADP eurjchem-29 87 8     SPACE eurjchem-29 87 9 c36h23n12o4s c36h23n12o4s PROPN eurjchem-29 87 10     SPACE eurjchem-29 87 11 ( ( PUNCT eurjchem-29 87 12 719 719 NUM eurjchem-29 87 13 ): ): PUNCT eurjchem-29 87 14     SPACE eurjchem-29 87 15 c c NOUN eurjchem-29 87 16 , , PUNCT eurjchem-29 87 17     SPACE eurjchem-29 87 18 58.41 58.41 NUM eurjchem-29 87 19 ; ; PUNCT eurjchem-29 87 20     SPACE eurjchem-29 87 21 h h NOUN eurjchem-29 87 22 , , PUNCT eurjchem-29 87 23     SPACE eurjchem-29 87 24 3.19 3.19 NUM eurjchem-29 87 25 ; ; PUNCT eurjchem-29 87 26     SPACE eurjchem-29 87 27 n n CCONJ eurjchem-29 87 28 , , PUNCT eurjchem-29 87 29     SPACE eurjchem-29 87 30 23.36 23.36 NUM eurjchem-29 87 31 ; ; PUNCT eurjchem-29 87 32     SPACE eurjchem-29 87 33 s s PROPN eurjchem-29 87 34 , , PUNCT eurjchem-29 87 35     SPACE eurjchem-29 87 36 4.45 4.45 NUM eurjchem-29 87 37 . . PUNCT eurjchem-29 87 38     SPACE eurjchem-29 87 39 found find VERB eurjchem-29 87 40 : : PUNCT eurjchem-29 87 41     SPACE eurjchem-29 87 42 c c X eurjchem-29 87 43 , , PUNCT eurjchem-29 87 44     SPACE eurjchem-29 87 45 58.64 58.64 NUM eurjchem-29 87 46 ; ; PUNCT eurjchem-29 87 47     SPACE eurjchem-29 87 48 h h NOUN eurjchem-29 87 49 , , PUNCT eurjchem-29 87 50     SPACE eurjchem-29 87 51 3.59 3.59 NUM eurjchem-29 87 52 ; ; PUNCT eurjchem-29 87 53     SPACE eurjchem-29 87 54 n n CCONJ eurjchem-29 87 55 , , PUNCT eurjchem-29 87 56     SPACE eurjchem-29 87 57 23.61 23.61 NUM eurjchem-29 87 58 ; ; PUNCT eurjchem-29 87 59     SPACE eurjchem-29 87 60 s s PROPN eurjchem-29 87 61 , , PUNCT eurjchem-29 87 62     SPACE eurjchem-29 87 63 4.66 4.66 NUM eurjchem-29 87 64 % % NOUN eurjchem-29 87 65 . . PUNCT eurjchem-29 87 66           SPACE eurjchem-29 88 1 2.2.8 2.2.8 NUM eurjchem-29 88 2 . . PUNCT eurjchem-29 88 3     SPACE eurjchem-29 89 1 ethyl­8­[5,6­diphenyl­4­(1,3­thiazol­2­yl)­1h­1,2,4­ ethyl­8­[5,6­diphenyl­4­(1,3­thiazol­2­yl)­1h­1,2,4­ NUM eurjchem-29 89 2 triazin­3­yl]­3[7­(4­chloro­phenyl)­6­cyano­5­oxo­ triazin­3­yl]­3[7­(4­chloro­phenyl)­6­cyano­5­oxo­ PROPN eurjchem-29 89 3 [ [ X eurjchem-29 89 4 1,2,4]triazolo[1,5­a]pyridine­8­yl]­1­acetate 1,2,4]triazolo[1,5­a]pyridine­8­yl]­1­acetate NUM eurjchem-29 89 5     SPACE eurjchem-29 89 6 ( ( PUNCT eurjchem-29 89 7 10 10 NUM eurjchem-29 89 8 ) ) PUNCT eurjchem-29 89 9         SPACE eurjchem-29 89 10 a a DET eurjchem-29 89 11     SPACE eurjchem-29 89 12 mixture mixture NOUN eurjchem-29 89 13     SPACE eurjchem-29 89 14 of of ADP eurjchem-29 89 15     SPACE eurjchem-29 89 16 compound compound NOUN eurjchem-29 89 17     SPACE eurjchem-29 89 18 6a 6a NOUN eurjchem-29 89 19     SPACE eurjchem-29 89 20 ( ( PUNCT eurjchem-29 89 21 0.01 0.01 NUM eurjchem-29 89 22     SPACE eurjchem-29 89 23 mol mol NOUN eurjchem-29 89 24 ) ) PUNCT eurjchem-29 89 25     SPACE eurjchem-29 89 26 and and CCONJ eurjchem-29 89 27     SPACE eurjchem-29 89 28 ethyl ethyl NOUN eurjchem-29 89 29     SPACE eurjchem-29 89 30 chloroacetate chloroacetate NOUN eurjchem-29 89 31     SPACE eurjchem-29 89 32 ( ( PUNCT eurjchem-29 89 33 0.01 0.01 NUM eurjchem-29 89 34     SPACE eurjchem-29 89 35 mol mol NOUN eurjchem-29 89 36 ) ) PUNCT eurjchem-29 89 37     SPACE eurjchem-29 89 38 in in ADP eurjchem-29 89 39     SPACE eurjchem-29 89 40 dmf dmf PROPN eurjchem-29 89 41     SPACE eurjchem-29 89 42 ( ( PUNCT eurjchem-29 89 43 20 20 NUM eurjchem-29 89 44     SPACE eurjchem-29 89 45 cm3 cm3 NOUN eurjchem-29 89 46 ) ) PUNCT eurjchem-29 89 47     SPACE eurjchem-29 89 48 was be AUX eurjchem-29 89 49     SPACE eurjchem-29 89 50 refluxed refluxe VERB eurjchem-29 89 51     SPACE eurjchem-29 89 52 for for ADP eurjchem-29 89 53     SPACE eurjchem-29 89 54 2 2 NUM eurjchem-29 89 55     SPACE eurjchem-29 89 56 h h NOUN eurjchem-29 89 57 , , PUNCT eurjchem-29 89 58     SPACE eurjchem-29 89 59 the the DET eurjchem-29 89 60     SPACE eurjchem-29 89 61 reaction reaction NOUN eurjchem-29 89 62     SPACE eurjchem-29 89 63 mixture mixture NOUN eurjchem-29 89 64     SPACE eurjchem-29 89 65 was be AUX eurjchem-29 89 66     SPACE eurjchem-29 89 67 poured pour VERB eurjchem-29 89 68     SPACE eurjchem-29 89 69 onto onto ADP eurjchem-29 89 70     SPACE eurjchem-29 89 71 crushed crushed ADJ eurjchem-29 89 72     SPACE eurjchem-29 89 73 ice ice NOUN eurjchem-29 89 74     SPACE eurjchem-29 89 75 and and CCONJ eurjchem-29 89 76     SPACE eurjchem-29 89 77 the the DET eurjchem-29 89 78     SPACE eurjchem-29 89 79 separated separate VERB eurjchem-29 89 80     SPACE eurjchem-29 89 81 solid solid NOUN eurjchem-29 89 82     SPACE eurjchem-29 89 83 was be AUX eurjchem-29 89 84     SPACE eurjchem-29 89 85 filtered filter VERB eurjchem-29 89 86     SPACE eurjchem-29 89 87 off off ADP eurjchem-29 89 88 , , PUNCT eurjchem-29 89 89     SPACE eurjchem-29 89 90 dried dry VERB eurjchem-29 89 91     SPACE eurjchem-29 89 92 and and CCONJ eurjchem-29 89 93     SPACE eurjchem-29 89 94 crystallized crystallize VERB eurjchem-29 89 95     SPACE eurjchem-29 89 96 from from ADP eurjchem-29 89 97     SPACE eurjchem-29 89 98 ethanol ethanol NOUN eurjchem-29 89 99     SPACE eurjchem-29 89 100 ( ( PUNCT eurjchem-29 89 101 scheme scheme NOUN eurjchem-29 89 102     SPACE eurjchem-29 89 103 2 2 NUM eurjchem-29 89 104 ) ) PUNCT eurjchem-29 89 105 . . PUNCT eurjchem-29 89 106     SPACE eurjchem-29 90 1 yield yield NOUN eurjchem-29 90 2 : : PUNCT eurjchem-29 90 3     SPACE eurjchem-29 90 4 74 74 NUM eurjchem-29 90 5     SPACE eurjchem-29 90 6 % % NOUN eurjchem-29 90 7 . . PUNCT eurjchem-29 90 8     SPACE eurjchem-29 91 1 m.p m.p PROPN eurjchem-29 91 2 . . PROPN eurjchem-29 91 3 : : PUNCT eurjchem-29 91 4     SPACE eurjchem-29 92 1 189‐192 189‐192 NUM eurjchem-29 92 2     SPACE eurjchem-29 92 3 ° ° PROPN eurjchem-29 92 4 c c NOUN eurjchem-29 92 5 . . PUNCT eurjchem-29 92 6     SPACE eurjchem-29 92 7 ft‐ ft‐ AUX eurjchem-29 92 8     SPACE eurjchem-29 92 9 ir ir VERB eurjchem-29 92 10     SPACE eurjchem-29 92 11 ( ( PUNCT eurjchem-29 92 12 kbr kbr PROPN eurjchem-29 92 13 ) ) PUNCT eurjchem-29 92 14     SPACE eurjchem-29 92 15 ν ν NOUN eurjchem-29 92 16 , , PUNCT eurjchem-29 92 17     SPACE eurjchem-29 92 18 ( ( PUNCT eurjchem-29 92 19 cm‐1 cm‐1 NOUN eurjchem-29 92 20 ): ): PUNCT eurjchem-29 92 21     SPACE eurjchem-29 92 22 3434 3434 NUM eurjchem-29 92 23     SPACE eurjchem-29 92 24 ( ( PUNCT eurjchem-29 92 25 nh nh NOUN eurjchem-29 92 26 ) ) PUNCT eurjchem-29 92 27 , , PUNCT eurjchem-29 92 28     SPACE eurjchem-29 92 29 2982 2982 NUM eurjchem-29 92 30     SPACE eurjchem-29 92 31 ( ( PUNCT eurjchem-29 92 32 ch2 ch2 PROPN eurjchem-29 92 33 ) ) PUNCT eurjchem-29 92 34 , , PUNCT eurjchem-29 92 35     SPACE eurjchem-29 92 36 2214 2214 NUM eurjchem-29 92 37     SPACE eurjchem-29 92 38 ( ( PUNCT eurjchem-29 92 39 c≡n c≡n PROPN eurjchem-29 92 40 ) ) PUNCT eurjchem-29 92 41 , , PUNCT eurjchem-29 92 42     SPACE eurjchem-29 92 43 1685 1685 NUM eurjchem-29 92 44 , , PUNCT eurjchem-29 92 45     SPACE eurjchem-29 92 46 1670 1670 NUM eurjchem-29 92 47     SPACE eurjchem-29 92 48 ( ( PUNCT eurjchem-29 92 49 2 2 NUM eurjchem-29 92 50     SPACE eurjchem-29 92 51 c c NOUN eurjchem-29 92 52 = = NOUN eurjchem-29 92 53 o o NOUN eurjchem-29 92 54 ) ) PUNCT eurjchem-29 92 55     SPACE eurjchem-29 92 56 1488 1488 NUM eurjchem-29 92 57     SPACE eurjchem-29 92 58 ( ( PUNCT eurjchem-29 92 59 def def ADJ eurjchem-29 92 60 . . PUNCT eurjchem-29 92 61     SPACE eurjchem-29 92 62 ch2 ch2 PROPN eurjchem-29 92 63 ) ) PUNCT eurjchem-29 92 64 , , PUNCT eurjchem-29 92 65     SPACE eurjchem-29 92 66 1556 1556 NUM eurjchem-29 92 67     SPACE eurjchem-29 92 68 ( ( PUNCT eurjchem-29 92 69 c c NOUN eurjchem-29 92 70 = = SYM eurjchem-29 92 71 n n NUM eurjchem-29 92 72 ) ) PUNCT eurjchem-29 92 73 , , PUNCT eurjchem-29 92 74     SPACE eurjchem-29 92 75 696 696 NUM eurjchem-29 92 76     SPACE eurjchem-29 92 77 ( ( PUNCT eurjchem-29 92 78 c c NOUN eurjchem-29 92 79 – – PUNCT eurjchem-29 92 80 cl cl NOUN eurjchem-29 92 81 ) ) PUNCT eurjchem-29 92 82 . . PUNCT eurjchem-29 92 83         SPACE eurjchem-29 93 1 1h 1h NUM eurjchem-29 93 2     SPACE eurjchem-29 93 3 nmr nmr NOUN eurjchem-29 93 4     SPACE eurjchem-29 93 5 ( ( PUNCT eurjchem-29 93 6 200 200 NUM eurjchem-29 93 7     SPACE eurjchem-29 93 8 mhz mhz NOUN eurjchem-29 93 9 , , PUNCT eurjchem-29 93 10     SPACE eurjchem-29 93 11 dmso‐d6 dmso‐d6 NOUN eurjchem-29 93 12 ) ) PUNCT eurjchem-29 93 13 , , PUNCT eurjchem-29 93 14     SPACE eurjchem-29 93 15 δ δ PROPN eurjchem-29 93 16 : : PUNCT eurjchem-29 93 17     SPACE eurjchem-29 93 18 1.55 1.55 NUM eurjchem-29 93 19     SPACE eurjchem-29 93 20 ( ( PUNCT eurjchem-29 93 21 t t PROPN eurjchem-29 93 22 , , PUNCT eurjchem-29 93 23     SPACE eurjchem-29 93 24 3h 3h NUM eurjchem-29 93 25 , , PUNCT eurjchem-29 93 26     SPACE eurjchem-29 93 27 ch3 ch3 PROPN eurjchem-29 93 28 ) ) PUNCT eurjchem-29 93 29 , , PUNCT eurjchem-29 93 30     SPACE eurjchem-29 93 31 3.97 3.97 NUM eurjchem-29 93 32     SPACE eurjchem-29 93 33 ( ( PUNCT eurjchem-29 93 34 s s PROPN eurjchem-29 93 35 , , PUNCT eurjchem-29 93 36     SPACE eurjchem-29 93 37 2h 2h NUM eurjchem-29 93 38 , , PUNCT eurjchem-29 93 39     SPACE eurjchem-29 93 40 ch2 ch2 NOUN eurjchem-29 93 41 ) ) PUNCT eurjchem-29 93 42 , , PUNCT eurjchem-29 93 43     SPACE eurjchem-29 93 44 7.25–7.96 7.25–7.96 NOUN eurjchem-29 93 45     SPACE eurjchem-29 93 46 ( ( PUNCT eurjchem-29 93 47 m m PROPN eurjchem-29 93 48 , , PUNCT eurjchem-29 93 49     SPACE eurjchem-29 93 50 17h 17h NOUN eurjchem-29 93 51 , , PUNCT eurjchem-29 93 52     SPACE eurjchem-29 93 53 ar‐h ar‐h NOUN eurjchem-29 93 54 ) ) PUNCT eurjchem-29 93 55 , , PUNCT eurjchem-29 93 56     SPACE eurjchem-29 93 57 9.78 9.78 NUM eurjchem-29 93 58     SPACE eurjchem-29 93 59 ( ( PUNCT eurjchem-29 93 60 s s PROPN eurjchem-29 93 61 , , PUNCT eurjchem-29 93 62     SPACE eurjchem-29 93 63 1h 1h NUM eurjchem-29 93 64 , , PUNCT eurjchem-29 93 65     SPACE eurjchem-29 93 66 nh nh PROPN eurjchem-29 93 67 ) ) PUNCT eurjchem-29 93 68 . . PUNCT eurjchem-29 93 69     SPACE eurjchem-29 94 1 anal anal ADJ eurjchem-29 94 2 . . PUNCT eurjchem-29 94 3     SPACE eurjchem-29 94 4 calcd calcd NOUN eurjchem-29 94 5 . . PUNCT eurjchem-29 94 6     SPACE eurjchem-29 95 1 for for ADP eurjchem-29 95 2     SPACE eurjchem-29 95 3 c35h25n8o3scl c35h25n8o3scl PROPN eurjchem-29 95 4     SPACE eurjchem-29 95 5 ( ( PUNCT eurjchem-29 95 6 672.5 672.5 NUM eurjchem-29 95 7 ): ): PUNCT eurjchem-29 95 8     SPACE eurjchem-29 95 9 c c NOUN eurjchem-29 95 10 , , PUNCT eurjchem-29 95 11     SPACE eurjchem-29 95 12 62.45 62.45 NUM eurjchem-29 95 13 ; ; PUNCT eurjchem-29 95 14     SPACE eurjchem-29 95 15 h h NOUN eurjchem-29 95 16 , , PUNCT eurjchem-29 95 17     SPACE eurjchem-29 95 18 3.71 3.71 NUM eurjchem-29 95 19 ; ; PUNCT eurjchem-29 95 20     SPACE eurjchem-29 95 21 n n CCONJ eurjchem-29 95 22 , , PUNCT eurjchem-29 95 23     SPACE eurjchem-29 95 24 16.65 16.65 NUM eurjchem-29 95 25 ; ; PUNCT eurjchem-29 95 26     SPACE eurjchem-29 95 27 s s PROPN eurjchem-29 95 28 , , PUNCT eurjchem-29 95 29     SPACE eurjchem-29 95 30 4.75 4.75 NUM eurjchem-29 95 31 ; ; PUNCT eurjchem-29 95 32     SPACE eurjchem-29 95 33 cl cl NOUN eurjchem-29 95 34 , , PUNCT eurjchem-29 95 35     SPACE eurjchem-29 95 36 5.27 5.27 NUM eurjchem-29 95 37 . . PUNCT eurjchem-29 95 38     SPACE eurjchem-29 95 39 found find VERB eurjchem-29 95 40 : : PUNCT eurjchem-29 95 41     SPACE eurjchem-29 95 42 c c X eurjchem-29 95 43 , , PUNCT eurjchem-29 95 44     SPACE eurjchem-29 95 45 62.09 62.09 NUM eurjchem-29 95 46 ; ; PUNCT eurjchem-29 95 47     SPACE eurjchem-29 95 48 h h NOUN eurjchem-29 95 49 , , PUNCT eurjchem-29 95 50     SPACE eurjchem-29 95 51 3.51 3.51 NUM eurjchem-29 95 52 ; ; PUNCT eurjchem-29 95 53     SPACE eurjchem-29 95 54 n n CCONJ eurjchem-29 95 55 , , PUNCT eurjchem-29 95 56     SPACE eurjchem-29 95 57 16.75 16.75 NUM eurjchem-29 95 58 ; ; PUNCT eurjchem-29 95 59     SPACE eurjchem-29 95 60 s s PROPN eurjchem-29 95 61 , , PUNCT eurjchem-29 95 62     SPACE eurjchem-29 95 63 4.51 4.51 NUM eurjchem-29 95 64 ; ; PUNCT eurjchem-29 95 65     SPACE eurjchem-29 95 66 cl cl NOUN eurjchem-29 95 67 , , PUNCT eurjchem-29 95 68     SPACE eurjchem-29 95 69 5.15 5.15 NUM eurjchem-29 95 70 % % NOUN eurjchem-29 95 71 . . PUNCT eurjchem-29 95 72           SPACE eurjchem-29 95 73 2.2.9 2.2.9 NUM eurjchem-29 95 74 . . PUNCT eurjchem-29 95 75     SPACE eurjchem-29 96 1 8­[5,6­diphenyl­4­(1,3­thiazol­2­yl)­1h­1,2,4­triazin­ 8­[5,6­diphenyl­4­(1,3­thiazol­2­yl)­1h­1,2,4­triazin­ NUM eurjchem-29 97 1 3yl]­3­[7­(4­chlorophenyl)­6­cyano­5­oxo[1,2,4]triazolo[1,5­ 3yl]­3­[7­(4­chlorophenyl)­6­cyano­5­oxo[1,2,4]triazolo[1,5­ NUM eurjchem-29 97 2 a]pyridine­8­yl)]1­carbohydrazide a]pyridine­8­yl)]1­carbohydrazide ADV eurjchem-29 97 3     SPACE eurjchem-29 97 4 ( ( PUNCT eurjchem-29 97 5 11 11 NUM eurjchem-29 97 6 ) ) PUNCT eurjchem-29 97 7         SPACE eurjchem-29 97 8 a a DET eurjchem-29 97 9     SPACE eurjchem-29 97 10 mixture mixture NOUN eurjchem-29 97 11     SPACE eurjchem-29 97 12 of of ADP eurjchem-29 97 13     SPACE eurjchem-29 97 14 compound compound NOUN eurjchem-29 97 15     SPACE eurjchem-29 97 16 10 10 NUM eurjchem-29 97 17     SPACE eurjchem-29 97 18 ( ( PUNCT eurjchem-29 97 19 0.01 0.01 NUM eurjchem-29 97 20     SPACE eurjchem-29 97 21 mol mol NOUN eurjchem-29 97 22 ) ) PUNCT eurjchem-29 97 23     SPACE eurjchem-29 97 24 and and CCONJ eurjchem-29 97 25     SPACE eurjchem-29 97 26 hydrazine hydrazine NOUN eurjchem-29 97 27     SPACE eurjchem-29 97 28 hydrate hydrate NOUN eurjchem-29 97 29     SPACE eurjchem-29 97 30 98 98 NUM eurjchem-29 97 31     SPACE eurjchem-29 97 32 % % NOUN eurjchem-29 97 33     SPACE eurjchem-29 97 34 ( ( PUNCT eurjchem-29 97 35 0.01 0.01 NUM eurjchem-29 97 36     SPACE eurjchem-29 97 37 mol mol NOUN eurjchem-29 97 38 ) ) PUNCT eurjchem-29 97 39     SPACE eurjchem-29 97 40 in in ADP eurjchem-29 97 41     SPACE eurjchem-29 97 42 absolute absolute ADJ eurjchem-29 97 43     SPACE eurjchem-29 97 44 ethanol ethanol NOUN eurjchem-29 97 45     SPACE eurjchem-29 97 46 ( ( PUNCT eurjchem-29 97 47 25 25 NUM eurjchem-29 97 48     SPACE eurjchem-29 97 49 cm3 cm3 NOUN eurjchem-29 97 50 ) ) PUNCT eurjchem-29 97 51         SPACE eurjchem-29 97 52 was be AUX eurjchem-29 97 53     SPACE eurjchem-29 97 54 refluxed refluxe VERB eurjchem-29 97 55     SPACE eurjchem-29 97 56 for for ADP eurjchem-29 97 57     SPACE eurjchem-29 97 58 2 2 NUM eurjchem-29 97 59     SPACE eurjchem-29 97 60 h h NOUN eurjchem-29 97 61 , , PUNCT eurjchem-29 97 62     SPACE eurjchem-29 97 63 the the DET eurjchem-29 97 64     SPACE eurjchem-29 97 65 reaction reaction NOUN eurjchem-29 97 66     SPACE eurjchem-29 97 67 mixture mixture NOUN eurjchem-29 97 68     SPACE eurjchem-29 97 69 was be AUX eurjchem-29 97 70     SPACE eurjchem-29 97 71 poured pour VERB eurjchem-29 97 72     SPACE eurjchem-29 97 73 onto onto ADP eurjchem-29 97 74     SPACE eurjchem-29 97 75 crushed crush VERB eurjchem-29 97 76     SPACE eurjchem-29 97 77 ice ice NOUN eurjchem-29 97 78     SPACE eurjchem-29 97 79 and and CCONJ eurjchem-29 97 80     SPACE eurjchem-29 97 81 the the DET eurjchem-29 97 82     SPACE eurjchem-29 97 83 separated separate VERB eurjchem-29 97 84     SPACE eurjchem-29 97 85 solid solid NOUN eurjchem-29 97 86     SPACE eurjchem-29 97 87 was be AUX eurjchem-29 97 88     SPACE eurjchem-29 97 89 filtered filter VERB eurjchem-29 97 90     SPACE eurjchem-29 97 91 off off ADP eurjchem-29 97 92 , , PUNCT eurjchem-29 97 93     SPACE eurjchem-29 97 94 dried dry VERB eurjchem-29 97 95     SPACE eurjchem-29 97 96 and and CCONJ eurjchem-29 97 97     SPACE eurjchem-29 97 98 crystallized crystallize VERB eurjchem-29 97 99     SPACE eurjchem-29 97 100 from from ADP eurjchem-29 97 101         SPACE eurjchem-29 97 102 a a DET eurjchem-29 97 103     SPACE eurjchem-29 97 104 mixture mixture NOUN eurjchem-29 97 105     SPACE eurjchem-29 97 106 of of ADP eurjchem-29 97 107     SPACE eurjchem-29 97 108 dmf dmf NOUN eurjchem-29 97 109     SPACE eurjchem-29 97 110 and and CCONJ eurjchem-29 97 111     SPACE eurjchem-29 97 112 water water NOUN eurjchem-29 97 113     SPACE eurjchem-29 97 114 ( ( PUNCT eurjchem-29 97 115 1:1 1:1 NUM eurjchem-29 97 116 ) ) PUNCT eurjchem-29 97 117     SPACE eurjchem-29 97 118 ( ( PUNCT eurjchem-29 97 119 scheme scheme NOUN eurjchem-29 97 120     SPACE eurjchem-29 97 121 2 2 NUM eurjchem-29 97 122 ) ) PUNCT eurjchem-29 97 123 . . PUNCT eurjchem-29 97 124     SPACE eurjchem-29 98 1 yield yield NOUN eurjchem-29 98 2 : : PUNCT eurjchem-29 98 3     SPACE eurjchem-29 98 4 69 69 NUM eurjchem-29 98 5 % % NOUN eurjchem-29 98 6 . . PUNCT eurjchem-29 98 7     SPACE eurjchem-29 99 1 m.p m.p PROPN eurjchem-29 99 2 . . PROPN eurjchem-29 99 3     SPACE eurjchem-29 99 4 > > PUNCT eurjchem-29 99 5     SPACE eurjchem-29 99 6 280 280 NUM eurjchem-29 99 7     SPACE eurjchem-29 99 8 ° ° NOUN eurjchem-29 99 9 c c NOUN eurjchem-29 99 10 . . PUNCT eurjchem-29 99 11     SPACE eurjchem-29 99 12 ft‐ ft‐ AUX eurjchem-29 99 13     SPACE eurjchem-29 99 14 ir ir VERB eurjchem-29 99 15     SPACE eurjchem-29 99 16 ( ( PUNCT eurjchem-29 99 17 kbr kbr PROPN eurjchem-29 99 18 ) ) PUNCT eurjchem-29 99 19     SPACE eurjchem-29 99 20 ν ν PROPN eurjchem-29 99 21 , , PUNCT eurjchem-29 99 22     SPACE eurjchem-29 99 23 ( ( PUNCT eurjchem-29 99 24 cm‐1 cm‐1 NOUN eurjchem-29 99 25 ): ): PUNCT eurjchem-29 99 26     SPACE eurjchem-29 99 27 3327 3327 NUM eurjchem-29 99 28 , , PUNCT eurjchem-29 99 29     SPACE eurjchem-29 99 30 3290 3290 NUM eurjchem-29 99 31     SPACE eurjchem-29 99 32 ( ( PUNCT eurjchem-29 99 33 nh2 nh2 PROPN eurjchem-29 99 34 ) ) PUNCT eurjchem-29 99 35 , , PUNCT eurjchem-29 99 36     SPACE eurjchem-29 99 37 3229 3229 NUM eurjchem-29 99 38     SPACE eurjchem-29 99 39 ( ( PUNCT eurjchem-29 99 40 nh nh NOUN eurjchem-29 99 41 ) ) PUNCT eurjchem-29 99 42 , , PUNCT eurjchem-29 99 43     SPACE eurjchem-29 99 44 3209 3209 NUM eurjchem-29 99 45     SPACE eurjchem-29 99 46 ( ( PUNCT eurjchem-29 99 47 nh nh NOUN eurjchem-29 99 48 ) ) PUNCT eurjchem-29 99 49 , , PUNCT eurjchem-29 99 50     SPACE eurjchem-29 99 51 3080 3080 NUM eurjchem-29 99 52     SPACE eurjchem-29 99 53 ( ( PUNCT eurjchem-29 99 54 ch2 ch2 PROPN eurjchem-29 99 55 ) ) PUNCT eurjchem-29 99 56 , , PUNCT eurjchem-29 99 57     SPACE eurjchem-29 99 58 2219 2219 NUM eurjchem-29 99 59     SPACE eurjchem-29 99 60 ( ( PUNCT eurjchem-29 99 61 c≡n c≡n PROPN eurjchem-29 99 62 ) ) PUNCT eurjchem-29 99 63 , , PUNCT eurjchem-29 99 64     SPACE eurjchem-29 99 65 1695 1695 NUM eurjchem-29 99 66 , , PUNCT eurjchem-29 99 67     SPACE eurjchem-29 99 68 1663 1663 NUM eurjchem-29 99 69     SPACE eurjchem-29 99 70 ( ( PUNCT eurjchem-29 99 71 2c 2c NOUN eurjchem-29 99 72 = = SYM eurjchem-29 99 73 o o NOUN eurjchem-29 99 74 ) ) PUNCT eurjchem-29 99 75 , , PUNCT eurjchem-29 99 76     SPACE eurjchem-29 99 77 776 776 NUM eurjchem-29 99 78     SPACE eurjchem-29 99 79 ( ( PUNCT eurjchem-29 99 80 c c NOUN eurjchem-29 99 81 – – PUNCT eurjchem-29 99 82 cl cl NOUN eurjchem-29 99 83 ) ) PUNCT eurjchem-29 99 84 . . PUNCT eurjchem-29 99 85     SPACE eurjchem-29 100 1 1h 1h NUM eurjchem-29 100 2     SPACE eurjchem-29 100 3 nmr nmr NOUN eurjchem-29 100 4     SPACE eurjchem-29 100 5 ( ( PUNCT eurjchem-29 100 6 200 200 NUM eurjchem-29 100 7     SPACE eurjchem-29 100 8 mhz mhz NOUN eurjchem-29 100 9 , , PUNCT eurjchem-29 100 10     SPACE eurjchem-29 100 11 dmso‐d6 dmso‐d6 NOUN eurjchem-29 100 12 ) ) PUNCT eurjchem-29 100 13 , , PUNCT eurjchem-29 100 14     SPACE eurjchem-29 100 15 δ δ PROPN eurjchem-29 100 16 : : PUNCT eurjchem-29 100 17     SPACE eurjchem-29 100 18 2.82 2.82 NUM eurjchem-29 100 19     SPACE eurjchem-29 100 20 abdel­monem abdel­monem NOUN eurjchem-29 100 21     SPACE eurjchem-29 100 22 / / SYM eurjchem-29 100 23     SPACE eurjchem-29 100 24 european european ADJ eurjchem-29 100 25     SPACE eurjchem-29 100 26 journal journal NOUN eurjchem-29 100 27     SPACE eurjchem-29 100 28 of of ADP eurjchem-29 100 29     SPACE eurjchem-29 100 30 chemistry chemistry NOUN eurjchem-29 100 31     SPACE eurjchem-29 100 32 1 1 NUM eurjchem-29 100 33     SPACE eurjchem-29 100 34 ( ( PUNCT eurjchem-29 100 35 3 3 NUM eurjchem-29 100 36 ) ) PUNCT eurjchem-29 100 37     SPACE eurjchem-29 100 38 ( ( PUNCT eurjchem-29 100 39 2010 2010 NUM eurjchem-29 100 40 ) ) PUNCT eurjchem-29 100 41     SPACE eurjchem-29 100 42 168­172 168­172 NUM eurjchem-29 100 43     SPACE eurjchem-29 100 44 171 171 NUM eurjchem-29 100 45     SPACE eurjchem-29 100 46 ( ( PUNCT eurjchem-29 100 47 s s PROPN eurjchem-29 100 48 , , PUNCT eurjchem-29 100 49     SPACE eurjchem-29 100 50 2h 2h NUM eurjchem-29 100 51 , , PUNCT eurjchem-29 100 52     SPACE eurjchem-29 100 53 ch2co ch2co NOUN eurjchem-29 100 54 ) ) PUNCT eurjchem-29 100 55 , , PUNCT eurjchem-29 100 56     SPACE eurjchem-29 100 57 5.72 5.72 NUM eurjchem-29 100 58     SPACE eurjchem-29 100 59 ( ( PUNCT eurjchem-29 100 60 s s PROPN eurjchem-29 100 61 , , PUNCT eurjchem-29 100 62     SPACE eurjchem-29 100 63 br br PROPN eurjchem-29 100 64 , , PUNCT eurjchem-29 100 65     SPACE eurjchem-29 100 66 2h 2h NUM eurjchem-29 100 67 , , PUNCT eurjchem-29 100 68     SPACE eurjchem-29 100 69 nh2 nh2 PROPN eurjchem-29 100 70 ) ) PUNCT eurjchem-29 100 71 , , PUNCT eurjchem-29 100 72     SPACE eurjchem-29 100 73 8.78 8.78 NUM eurjchem-29 100 74     SPACE eurjchem-29 100 75 ( ( PUNCT eurjchem-29 100 76 s s PROPN eurjchem-29 100 77 , , PUNCT eurjchem-29 100 78     SPACE eurjchem-29 100 79 1h 1h NUM eurjchem-29 100 80 , , PUNCT eurjchem-29 100 81     SPACE eurjchem-29 100 82 nh nh PROPN eurjchem-29 100 83 ) ) PUNCT eurjchem-29 100 84 , , PUNCT eurjchem-29 100 85     SPACE eurjchem-29 100 86 9.25 9.25 NUM eurjchem-29 100 87     SPACE eurjchem-29 100 88 ( ( PUNCT eurjchem-29 100 89 s s PROPN eurjchem-29 100 90 , , PUNCT eurjchem-29 100 91     SPACE eurjchem-29 100 92 1h 1h NUM eurjchem-29 100 93 , , PUNCT eurjchem-29 100 94     SPACE eurjchem-29 100 95 nh nh PROPN eurjchem-29 100 96 ) ) PUNCT eurjchem-29 100 97 . . PUNCT eurjchem-29 100 98     SPACE eurjchem-29 101 1 anal anal ADJ eurjchem-29 101 2 . . PUNCT eurjchem-29 101 3     SPACE eurjchem-29 101 4 calcd calcd NOUN eurjchem-29 101 5 . . PUNCT eurjchem-29 101 6     SPACE eurjchem-29 101 7 for for ADP eurjchem-29 101 8     SPACE eurjchem-29 101 9 c33h23n10o2scl c33h23n10o2scl NOUN eurjchem-29 101 10     SPACE eurjchem-29 101 11 ( ( PUNCT eurjchem-29 101 12 658.5 658.5 NUM eurjchem-29 101 13 ): ): SYM eurjchem-29 101 14     SPACE eurjchem-29 101 15 c c NOUN eurjchem-29 101 16 , , PUNCT eurjchem-29 101 17     SPACE eurjchem-29 101 18 60.13 60.13 NUM eurjchem-29 101 19 ; ; PUNCT eurjchem-29 101 20     SPACE eurjchem-29 101 21 h h NOUN eurjchem-29 101 22 , , PUNCT eurjchem-29 101 23     SPACE eurjchem-29 101 24 3.49 3.49 NUM eurjchem-29 101 25 ; ; PUNCT eurjchem-29 101 26     SPACE eurjchem-29 101 27 n n CCONJ eurjchem-29 101 28 , , PUNCT eurjchem-29 101 29     SPACE eurjchem-29 101 30 21.26 21.26 NUM eurjchem-29 101 31 ; ; PUNCT eurjchem-29 101 32     SPACE eurjchem-29 101 33 s s PROPN eurjchem-29 101 34 , , PUNCT eurjchem-29 101 35     SPACE eurjchem-29 101 36 4.85 4.85 NUM eurjchem-29 101 37 ; ; PUNCT eurjchem-29 101 38     SPACE eurjchem-29 101 39 cl cl NOUN eurjchem-29 101 40 , , PUNCT eurjchem-29 101 41     SPACE eurjchem-29 101 42 5.39 5.39 NUM eurjchem-29 101 43 . . PUNCT eurjchem-29 101 44     SPACE eurjchem-29 101 45 found find VERB eurjchem-29 101 46 : : PUNCT eurjchem-29 101 47     SPACE eurjchem-29 101 48 c c X eurjchem-29 101 49 , , PUNCT eurjchem-29 101 50     SPACE eurjchem-29 101 51 60.48 60.48 NUM eurjchem-29 101 52 ; ; PUNCT eurjchem-29 101 53     SPACE eurjchem-29 101 54 h h NOUN eurjchem-29 101 55 , , PUNCT eurjchem-29 101 56     SPACE eurjchem-29 101 57 3.84 3.84 NUM eurjchem-29 101 58 ; ; PUNCT eurjchem-29 101 59     SPACE eurjchem-29 101 60 n n CCONJ eurjchem-29 101 61 , , PUNCT eurjchem-29 101 62     SPACE eurjchem-29 101 63 21.52 21.52 NUM eurjchem-29 101 64 ; ; PUNCT eurjchem-29 101 65     SPACE eurjchem-29 101 66 s s PROPN eurjchem-29 101 67 , , PUNCT eurjchem-29 101 68     SPACE eurjchem-29 101 69 5.21 5.21 NUM eurjchem-29 101 70 ; ; PUNCT eurjchem-29 101 71     SPACE eurjchem-29 101 72 cl cl NOUN eurjchem-29 101 73 , , PUNCT eurjchem-29 101 74     SPACE eurjchem-29 101 75 5.64 5.64 NUM eurjchem-29 101 76 % % NOUN eurjchem-29 101 77 . . PUNCT eurjchem-29 101 78         SPACE eurjchem-29 102 1 2.2.10 2.2.10 NUM eurjchem-29 102 2 . . PUNCT eurjchem-29 102 3     SPACE eurjchem-29 102 4 8­[5,6­diphenyl­4­(1,3­thiazol­2­yl)­1,2,4­triazin­3­ 8­[5,6­diphenyl­4­(1,3­thiazol­2­yl)­1,2,4­triazin­3­ PROPN eurjchem-29 102 5 yl]­3­(7­(4­chloro­phenyl)­6­cyano­5­oxo[1,2,4]triazolo[1,5­ yl]­3­(7­(4­chloro­phenyl)­6­cyano­5­oxo[1,2,4]triazolo[1,5­ PROPN eurjchem-29 102 6 a]pyridine­8­yl)­1­carbonyl­methylhydrazinecarbo a]pyridine­8­yl)­1­carbonyl­methylhydrazinecarbo PROPN eurjchem-29 102 7     SPACE eurjchem-29 102 8 thioamide thioamide NOUN eurjchem-29 102 9     SPACE eurjchem-29 102 10 ( ( PUNCT eurjchem-29 102 11 12 12 NUM eurjchem-29 102 12 ) ) PUNCT eurjchem-29 102 13         SPACE eurjchem-29 102 14 a a DET eurjchem-29 102 15     SPACE eurjchem-29 102 16 mixture mixture NOUN eurjchem-29 102 17     SPACE eurjchem-29 102 18 of of ADP eurjchem-29 102 19     SPACE eurjchem-29 102 20 compound compound NOUN eurjchem-29 102 21     SPACE eurjchem-29 102 22 11 11 NUM eurjchem-29 102 23     SPACE eurjchem-29 102 24 ( ( PUNCT eurjchem-29 102 25 0.01 0.01 NUM eurjchem-29 102 26     SPACE eurjchem-29 102 27 mol mol NOUN eurjchem-29 102 28 ) ) PUNCT eurjchem-29 102 29     SPACE eurjchem-29 102 30 and and CCONJ eurjchem-29 102 31     SPACE eurjchem-29 102 32 ammonium ammonium NOUN eurjchem-29 102 33     SPACE eurjchem-29 102 34 thiocyanate thiocyanate NOUN eurjchem-29 102 35     SPACE eurjchem-29 102 36 ( ( PUNCT eurjchem-29 102 37 0.01 0.01 NUM eurjchem-29 102 38     SPACE eurjchem-29 102 39 mol mol NOUN eurjchem-29 102 40 ) ) PUNCT eurjchem-29 102 41     SPACE eurjchem-29 102 42 in in ADP eurjchem-29 102 43     SPACE eurjchem-29 102 44 ethanol ethanol NOUN eurjchem-29 102 45     SPACE eurjchem-29 102 46 ( ( PUNCT eurjchem-29 102 47 20 20 NUM eurjchem-29 102 48     SPACE eurjchem-29 102 49 cm3 cm3 NOUN eurjchem-29 102 50 ) ) PUNCT eurjchem-29 102 51     SPACE eurjchem-29 102 52 and and CCONJ eurjchem-29 102 53     SPACE eurjchem-29 102 54 hcl hcl PROPN eurjchem-29 102 55     SPACE eurjchem-29 102 56 ( ( PUNCT eurjchem-29 102 57 3 3 NUM eurjchem-29 102 58     SPACE eurjchem-29 102 59 cm3 cm3 NOUN eurjchem-29 102 60 ) ) PUNCT eurjchem-29 102 61     SPACE eurjchem-29 102 62 was be AUX eurjchem-29 102 63     SPACE eurjchem-29 102 64 refluxed refluxe VERB eurjchem-29 102 65     SPACE eurjchem-29 102 66 for for ADP eurjchem-29 102 67     SPACE eurjchem-29 102 68 4 4 NUM eurjchem-29 102 69     SPACE eurjchem-29 102 70 h h NOUN eurjchem-29 102 71     SPACE eurjchem-29 102 72 and and CCONJ eurjchem-29 102 73     SPACE eurjchem-29 102 74 then then ADV eurjchem-29 102 75     SPACE eurjchem-29 102 76 allowed allow VERB eurjchem-29 102 77     SPACE eurjchem-29 102 78 to to PART eurjchem-29 102 79     SPACE eurjchem-29 102 80 cool cool ADJ eurjchem-29 102 81 . . PUNCT eurjchem-29 102 82     SPACE eurjchem-29 103 1 the the DET eurjchem-29 103 2     SPACE eurjchem-29 103 3 precipitate precipitate NOUN eurjchem-29 103 4     SPACE eurjchem-29 103 5 that that PRON eurjchem-29 103 6     SPACE eurjchem-29 103 7 formed form VERB eurjchem-29 103 8     SPACE eurjchem-29 103 9 was be AUX eurjchem-29 103 10     SPACE eurjchem-29 103 11 filtered filter VERB eurjchem-29 103 12     SPACE eurjchem-29 103 13 off off ADP eurjchem-29 103 14 , , PUNCT eurjchem-29 103 15     SPACE eurjchem-29 103 16 dried dry VERB eurjchem-29 103 17     SPACE eurjchem-29 103 18 and and CCONJ eurjchem-29 103 19     SPACE eurjchem-29 103 20 crystallized crystallize VERB eurjchem-29 103 21     SPACE eurjchem-29 103 22 from from ADP eurjchem-29 103 23     SPACE eurjchem-29 103 24 dmf dmf PROPN eurjchem-29 103 25     SPACE eurjchem-29 103 26 ( ( PUNCT eurjchem-29 103 27 scheme scheme NOUN eurjchem-29 103 28     SPACE eurjchem-29 103 29 2 2 NUM eurjchem-29 103 30 ) ) PUNCT eurjchem-29 103 31 . . PUNCT eurjchem-29 103 32     SPACE eurjchem-29 103 33 yield yield NOUN eurjchem-29 103 34 : : PUNCT eurjchem-29 103 35     SPACE eurjchem-29 103 36 80 80 NUM eurjchem-29 103 37 % % NOUN eurjchem-29 103 38 . . PUNCT eurjchem-29 103 39     SPACE eurjchem-29 104 1 m.p m.p PROPN eurjchem-29 104 2 . . PROPN eurjchem-29 104 3 : : PUNCT eurjchem-29 104 4     SPACE eurjchem-29 104 5 257‐259 257‐259 NOUN eurjchem-29 104 6     SPACE eurjchem-29 104 7 ° ° PROPN eurjchem-29 104 8 c c NOUN eurjchem-29 104 9 . . PUNCT eurjchem-29 104 10     SPACE eurjchem-29 105 1 ft‐ ft‐ PROPN eurjchem-29 105 2     SPACE eurjchem-29 105 3 ir ir PROPN eurjchem-29 105 4     SPACE eurjchem-29 105 5 ( ( PUNCT eurjchem-29 105 6 kbr kbr PROPN eurjchem-29 105 7 ) ) PUNCT eurjchem-29 105 8     SPACE eurjchem-29 105 9 ν ν NOUN eurjchem-29 105 10 , , PUNCT eurjchem-29 105 11               SPACE eurjchem-29 105 12 ( ( PUNCT eurjchem-29 105 13 cm‐1 cm‐1 NOUN eurjchem-29 105 14 ): ): PUNCT eurjchem-29 105 15     SPACE eurjchem-29 105 16 3385 3385 NUM eurjchem-29 105 17 , , PUNCT eurjchem-29 105 18     SPACE eurjchem-29 105 19 3289 3289 NUM eurjchem-29 105 20     SPACE eurjchem-29 105 21 ( ( PUNCT eurjchem-29 105 22 nh2 nh2 PROPN eurjchem-29 105 23 ) ) PUNCT eurjchem-29 105 24 , , PUNCT eurjchem-29 105 25     SPACE eurjchem-29 105 26 3266 3266 NUM eurjchem-29 105 27 , , PUNCT eurjchem-29 105 28     SPACE eurjchem-29 105 29 3184 3184 NUM eurjchem-29 105 30 , , PUNCT eurjchem-29 105 31     SPACE eurjchem-29 105 32 3147 3147 NUM eurjchem-29 105 33     SPACE eurjchem-29 105 34 ( ( PUNCT eurjchem-29 105 35 3 3 NUM eurjchem-29 105 36     SPACE eurjchem-29 105 37 nh nh PROPN eurjchem-29 105 38 ) ) PUNCT eurjchem-29 105 39 , , PUNCT eurjchem-29 105 40     SPACE eurjchem-29 105 41 2991 2991 NUM eurjchem-29 105 42     SPACE eurjchem-29 105 43 ( ( PUNCT eurjchem-29 105 44 ch2 ch2 PROPN eurjchem-29 105 45 ) ) PUNCT eurjchem-29 105 46 , , PUNCT eurjchem-29 105 47     SPACE eurjchem-29 105 48 2214 2214 NUM eurjchem-29 105 49     SPACE eurjchem-29 105 50 ( ( PUNCT eurjchem-29 105 51 c≡n c≡n PROPN eurjchem-29 105 52 ) ) PUNCT eurjchem-29 105 53 , , PUNCT eurjchem-29 105 54     SPACE eurjchem-29 105 55 1686 1686 NUM eurjchem-29 105 56 , , PUNCT eurjchem-29 105 57     SPACE eurjchem-29 105 58 1653 1653 NUM eurjchem-29 105 59     SPACE eurjchem-29 105 60 ( ( PUNCT eurjchem-29 105 61 2c 2c NOUN eurjchem-29 105 62 = = SYM eurjchem-29 105 63 o o NOUN eurjchem-29 105 64 ) ) PUNCT eurjchem-29 105 65 , , PUNCT eurjchem-29 105 66     SPACE eurjchem-29 105 67 1623 1623 NUM eurjchem-29 105 68     SPACE eurjchem-29 105 69 ( ( PUNCT eurjchem-29 105 70 def def PROPN eurjchem-29 105 71 . . PUNCT eurjchem-29 105 72     SPACE eurjchem-29 105 73 nh2 nh2 PROPN eurjchem-29 105 74 ) ) PUNCT eurjchem-29 105 75 , , PUNCT eurjchem-29 105 76     SPACE eurjchem-29 105 77 1590 1590 NUM eurjchem-29 105 78     SPACE eurjchem-29 105 79 ( ( PUNCT eurjchem-29 105 80 c c NOUN eurjchem-29 105 81 = = SYM eurjchem-29 105 82 n n NUM eurjchem-29 105 83 ) ) PUNCT eurjchem-29 105 84 , , PUNCT eurjchem-29 105 85     SPACE eurjchem-29 105 86 1484 1484 NUM eurjchem-29 105 87     SPACE eurjchem-29 105 88 ( ( PUNCT eurjchem-29 105 89 def def ADJ eurjchem-29 105 90 . . PUNCT eurjchem-29 105 91     SPACE eurjchem-29 105 92 nh2 nh2 PROPN eurjchem-29 105 93 ) ) PUNCT eurjchem-29 105 94 , , PUNCT eurjchem-29 105 95     SPACE eurjchem-29 105 96 1237 1237 NUM eurjchem-29 105 97     SPACE eurjchem-29 105 98 ( ( PUNCT eurjchem-29 105 99 c c X eurjchem-29 105 100 = = SYM eurjchem-29 105 101 s s NOUN eurjchem-29 105 102 ) ) PUNCT eurjchem-29 105 103 , , PUNCT eurjchem-29 105 104     SPACE eurjchem-29 105 105 765 765 NUM eurjchem-29 105 106     SPACE eurjchem-29 105 107 ( ( PUNCT eurjchem-29 105 108 c c NOUN eurjchem-29 105 109 – – PUNCT eurjchem-29 105 110 cl cl NOUN eurjchem-29 105 111 ) ) PUNCT eurjchem-29 105 112 . . PUNCT eurjchem-29 105 113     SPACE eurjchem-29 106 1 1h 1h NUM eurjchem-29 106 2     SPACE eurjchem-29 106 3 nmr nmr NOUN eurjchem-29 106 4     SPACE eurjchem-29 106 5 ( ( PUNCT eurjchem-29 106 6 200 200 NUM eurjchem-29 106 7     SPACE eurjchem-29 106 8 mhz mhz NOUN eurjchem-29 106 9 , , PUNCT eurjchem-29 106 10     SPACE eurjchem-29 106 11 dmso‐d6 dmso‐d6 NOUN eurjchem-29 106 12 ) ) PUNCT eurjchem-29 106 13 , , PUNCT eurjchem-29 106 14     SPACE eurjchem-29 106 15 δ δ PROPN eurjchem-29 106 16 : : PUNCT eurjchem-29 106 17     SPACE eurjchem-29 106 18 3.87 3.87 NUM eurjchem-29 106 19     SPACE eurjchem-29 106 20 ( ( PUNCT eurjchem-29 106 21 s s PROPN eurjchem-29 106 22 , , PUNCT eurjchem-29 106 23     SPACE eurjchem-29 106 24 2h 2h NUM eurjchem-29 106 25 , , PUNCT eurjchem-29 106 26     SPACE eurjchem-29 106 27 ch2co ch2co NOUN eurjchem-29 106 28 ) ) PUNCT eurjchem-29 106 29 , , PUNCT eurjchem-29 106 30     SPACE eurjchem-29 106 31 4.94 4.94 NUM eurjchem-29 106 32     SPACE eurjchem-29 106 33 ( ( PUNCT eurjchem-29 106 34 s s PROPN eurjchem-29 106 35 , , PUNCT eurjchem-29 106 36     SPACE eurjchem-29 106 37 br br PROPN eurjchem-29 106 38 , , PUNCT eurjchem-29 106 39     SPACE eurjchem-29 106 40 2h 2h NUM eurjchem-29 106 41 , , PUNCT eurjchem-29 106 42     SPACE eurjchem-29 106 43 nh2 nh2 PROPN eurjchem-29 106 44 ) ) PUNCT eurjchem-29 106 45 , , PUNCT eurjchem-29 106 46     SPACE eurjchem-29 106 47 7.25 7.25 NUM eurjchem-29 106 48 – – PUNCT eurjchem-29 106 49 8.35 8.35 NUM eurjchem-29 106 50     SPACE eurjchem-29 106 51 ( ( PUNCT eurjchem-29 106 52 m m PROPN eurjchem-29 106 53 , , PUNCT eurjchem-29 106 54     SPACE eurjchem-29 106 55 22h 22h NOUN eurjchem-29 106 56 , , PUNCT eurjchem-29 106 57     SPACE eurjchem-29 106 58 ar‐h ar‐h NOUN eurjchem-29 106 59 ) ) PUNCT eurjchem-29 106 60 , , PUNCT eurjchem-29 106 61     SPACE eurjchem-29 106 62 7.98 7.98 NUM eurjchem-29 106 63     SPACE eurjchem-29 106 64 ( ( PUNCT eurjchem-29 106 65 s s PROPN eurjchem-29 106 66 , , PUNCT eurjchem-29 106 67     SPACE eurjchem-29 106 68 1h 1h NUM eurjchem-29 106 69 , , PUNCT eurjchem-29 106 70     SPACE eurjchem-29 106 71 nh nh PROPN eurjchem-29 106 72 ) ) PUNCT eurjchem-29 106 73 , , PUNCT eurjchem-29 106 74     SPACE eurjchem-29 106 75 8.88 8.88 NUM eurjchem-29 106 76     SPACE eurjchem-29 106 77 ( ( PUNCT eurjchem-29 106 78 s s PROPN eurjchem-29 106 79 , , PUNCT eurjchem-29 106 80     SPACE eurjchem-29 106 81 1h 1h NUM eurjchem-29 106 82 , , PUNCT eurjchem-29 106 83     SPACE eurjchem-29 106 84 nh nh PROPN eurjchem-29 106 85 ) ) PUNCT eurjchem-29 106 86 , , PUNCT eurjchem-29 106 87     SPACE eurjchem-29 106 88 9.12 9.12 NUM eurjchem-29 106 89     SPACE eurjchem-29 106 90 ( ( PUNCT eurjchem-29 106 91 s s PROPN eurjchem-29 106 92 , , PUNCT eurjchem-29 106 93     SPACE eurjchem-29 106 94 1h 1h NUM eurjchem-29 106 95 , , PUNCT eurjchem-29 106 96     SPACE eurjchem-29 106 97 nh nh PROPN eurjchem-29 106 98 ) ) PUNCT eurjchem-29 106 99 . . PUNCT eurjchem-29 106 100     SPACE eurjchem-29 107 1 anal.calcd anal.calcd PROPN eurjchem-29 107 2 . . PROPN eurjchem-29 107 3     SPACE eurjchem-29 107 4 for for ADP eurjchem-29 107 5     SPACE eurjchem-29 107 6 c34h24n11o2s2cl c34h24n11o2s2cl PROPN eurjchem-29 107 7     SPACE eurjchem-29 107 8 ( ( PUNCT eurjchem-29 107 9 717.5 717.5 NUM eurjchem-29 107 10 ): ): PUNCT eurjchem-29 107 11     SPACE eurjchem-29 107 12 c c NOUN eurjchem-29 107 13 , , PUNCT eurjchem-29 107 14     SPACE eurjchem-29 107 15 56.86 56.86 NUM eurjchem-29 107 16 ; ; PUNCT eurjchem-29 107 17     SPACE eurjchem-29 107 18 h h NOUN eurjchem-29 107 19 , , PUNCT eurjchem-29 107 20     SPACE eurjchem-29 107 21 3.34 3.34 NUM eurjchem-29 107 22 ; ; PUNCT eurjchem-29 107 23     SPACE eurjchem-29 107 24 n n CCONJ eurjchem-29 107 25 , , PUNCT eurjchem-29 107 26     SPACE eurjchem-29 107 27 21.46 21.46 NUM eurjchem-29 107 28 ; ; PUNCT eurjchem-29 107 29     SPACE eurjchem-29 107 30 s s PROPN eurjchem-29 107 31 , , PUNCT eurjchem-29 107 32     SPACE eurjchem-29 107 33 8.91 8.91 NUM eurjchem-29 107 34     SPACE eurjchem-29 107 35 cl cl NOUN eurjchem-29 107 36 , , PUNCT eurjchem-29 107 37     SPACE eurjchem-29 107 38 4.94 4.94 NUM eurjchem-29 107 39 . . PUNCT eurjchem-29 107 40     SPACE eurjchem-29 107 41 found find VERB eurjchem-29 107 42 : : PUNCT eurjchem-29 107 43     SPACE eurjchem-29 107 44 c c X eurjchem-29 107 45 , , PUNCT eurjchem-29 107 46     SPACE eurjchem-29 107 47 56.52 56.52 NUM eurjchem-29 107 48 ; ; PUNCT eurjchem-29 107 49     SPACE eurjchem-29 107 50 h h NOUN eurjchem-29 107 51 , , PUNCT eurjchem-29 107 52     SPACE eurjchem-29 107 53 3.59 3.59 NUM eurjchem-29 107 54 ; ; PUNCT eurjchem-29 107 55     SPACE eurjchem-29 107 56 n n CCONJ eurjchem-29 107 57 , , PUNCT eurjchem-29 107 58     SPACE eurjchem-29 107 59 21.80 21.80 NUM eurjchem-29 107 60 ; ; PUNCT eurjchem-29 107 61     SPACE eurjchem-29 107 62 s s PROPN eurjchem-29 107 63 , , PUNCT eurjchem-29 107 64     SPACE eurjchem-29 107 65 8.49 8.49 NUM eurjchem-29 107 66 ; ; PUNCT eurjchem-29 107 67     SPACE eurjchem-29 107 68 cl cl NOUN eurjchem-29 107 69 , , PUNCT eurjchem-29 107 70     SPACE eurjchem-29 107 71 4.70 4.70 NUM eurjchem-29 107 72 % % NOUN eurjchem-29 107 73 . . PUNCT eurjchem-29 107 74         SPACE eurjchem-29 108 1 2.2.11 2.2.11 NUM eurjchem-29 108 2 . . PUNCT eurjchem-29 108 3     SPACE eurjchem-29 109 1 7­(4­chlorophenyl)­8­[5,6­diphenyl­4­(1,3­thiazol­2­ 7­(4­chlorophenyl)­8­[5,6­diphenyl­4­(1,3­thiazol­2­ NUM eurjchem-29 109 2 yl)­1h­1,2,4­triazin­3­yl]­1­[(5­thioxo­2,5­dihydro­1h­1,2,4­ yl)­1h­1,2,4­triazin­3­yl]­1­[(5­thioxo­2,5­dihydro­1h­1,2,4­ PROPN eurjchem-29 109 3 trazolo­3­yl)methyl]­5­oxo[1,2,4]triazolo[1,5­a trazolo­3­yl)methyl]­5­oxo[1,2,4]triazolo[1,5­a NOUN eurjchem-29 109 4 ] ] SYM eurjchem-29 109 5     SPACE eurjchem-29 109 6 pyridine­6­ pyridine­6­ NOUN eurjchem-29 109 7 carbonitrile carbonitrile VERB eurjchem-29 109 8     SPACE eurjchem-29 109 9 ( ( PUNCT eurjchem-29 109 10 13 13 NUM eurjchem-29 109 11 ) ) PUNCT eurjchem-29 109 12         SPACE eurjchem-29 109 13 a a DET eurjchem-29 109 14     SPACE eurjchem-29 109 15 suspension suspension NOUN eurjchem-29 109 16     SPACE eurjchem-29 109 17 of of ADP eurjchem-29 109 18     SPACE eurjchem-29 109 19 12 12 NUM eurjchem-29 109 20     SPACE eurjchem-29 109 21 ( ( PUNCT eurjchem-29 109 22 0.01 0.01 NUM eurjchem-29 109 23     SPACE eurjchem-29 109 24 mol mol NOUN eurjchem-29 109 25 ) ) PUNCT eurjchem-29 109 26     SPACE eurjchem-29 109 27 in in ADP eurjchem-29 109 28     SPACE eurjchem-29 109 29 glacial glacial ADJ eurjchem-29 109 30     SPACE eurjchem-29 109 31 acetic acetic ADJ eurjchem-29 109 32     SPACE eurjchem-29 109 33 acid acid NOUN eurjchem-29 109 34     SPACE eurjchem-29 109 35 ( ( PUNCT eurjchem-29 109 36 30 30 NUM eurjchem-29 109 37     SPACE eurjchem-29 109 38 cm3 cm3 NOUN eurjchem-29 109 39 ) ) PUNCT eurjchem-29 109 40     SPACE eurjchem-29 109 41 and and CCONJ eurjchem-29 109 42     SPACE eurjchem-29 109 43 fused fuse VERB eurjchem-29 109 44     SPACE eurjchem-29 109 45 sodium sodium NOUN eurjchem-29 109 46     SPACE eurjchem-29 109 47 acetate acetate NOUN eurjchem-29 109 48     SPACE eurjchem-29 109 49 ( ( PUNCT eurjchem-29 109 50 3 3 NUM eurjchem-29 109 51     SPACE eurjchem-29 109 52 g g NOUN eurjchem-29 109 53 ) ) PUNCT eurjchem-29 109 54     SPACE eurjchem-29 109 55 was be AUX eurjchem-29 109 56     SPACE eurjchem-29 109 57 heated heated ADJ eurjchem-29 109 58     SPACE eurjchem-29 109 59 under under ADP eurjchem-29 109 60     SPACE eurjchem-29 109 61 reflux reflux NOUN eurjchem-29 109 62     SPACE eurjchem-29 109 63 for for ADP eurjchem-29 109 64     SPACE eurjchem-29 109 65 4h 4h NOUN eurjchem-29 109 66 , , PUNCT eurjchem-29 109 67     SPACE eurjchem-29 109 68 cooled cool VERB eurjchem-29 109 69     SPACE eurjchem-29 109 70 and and CCONJ eurjchem-29 109 71     SPACE eurjchem-29 109 72 poured pour VERB eurjchem-29 109 73     SPACE eurjchem-29 109 74 onto onto ADP eurjchem-29 109 75     SPACE eurjchem-29 109 76 crushed crush VERB eurjchem-29 109 77     SPACE eurjchem-29 109 78 ice ice NOUN eurjchem-29 109 79 . . PUNCT eurjchem-29 109 80     SPACE eurjchem-29 110 1 the the DET eurjchem-29 110 2     SPACE eurjchem-29 110 3 formed form VERB eurjchem-29 110 4     SPACE eurjchem-29 110 5 solid solid ADJ eurjchem-29 110 6     SPACE eurjchem-29 110 7 product product NOUN eurjchem-29 110 8     SPACE eurjchem-29 110 9 was be AUX eurjchem-29 110 10     SPACE eurjchem-29 110 11 collected collect VERB eurjchem-29 110 12     SPACE eurjchem-29 110 13 by by ADP eurjchem-29 110 14     SPACE eurjchem-29 110 15 filtration filtration NOUN eurjchem-29 110 16 , , PUNCT eurjchem-29 110 17     SPACE eurjchem-29 110 18 dried dry VERB eurjchem-29 110 19     SPACE eurjchem-29 110 20 and and CCONJ eurjchem-29 110 21     SPACE eurjchem-29 110 22 crystallized crystallize VERB eurjchem-29 110 23     SPACE eurjchem-29 110 24 from from ADP eurjchem-29 110 25     SPACE eurjchem-29 110 26 methanol methanol NOUN eurjchem-29 110 27     SPACE eurjchem-29 110 28 ( ( PUNCT eurjchem-29 110 29 scheme scheme NOUN eurjchem-29 110 30     SPACE eurjchem-29 110 31 2 2 NUM eurjchem-29 110 32 ) ) PUNCT eurjchem-29 110 33 . . PUNCT eurjchem-29 110 34     SPACE eurjchem-29 110 35 yield yield NOUN eurjchem-29 110 36 : : PUNCT eurjchem-29 110 37     SPACE eurjchem-29 110 38 60 60 NUM eurjchem-29 110 39 % % NOUN eurjchem-29 110 40 . . PUNCT eurjchem-29 110 41     SPACE eurjchem-29 111 1 m.p m.p PROPN eurjchem-29 111 2 . . PROPN eurjchem-29 111 3 : : PUNCT eurjchem-29 111 4     SPACE eurjchem-29 111 5 259‐262 259‐262 NUM eurjchem-29 111 6     SPACE eurjchem-29 111 7 ° ° PROPN eurjchem-29 111 8 c c NOUN eurjchem-29 111 9 . . PUNCT eurjchem-29 111 10     SPACE eurjchem-29 111 11 ft‐ ft‐ PROPN eurjchem-29 111 12     SPACE eurjchem-29 111 13 ir ir PROPN eurjchem-29 111 14     SPACE eurjchem-29 111 15 ( ( PUNCT eurjchem-29 111 16 kbr kbr PROPN eurjchem-29 111 17 ) ) PUNCT eurjchem-29 111 18     SPACE eurjchem-29 111 19 ν ν NOUN eurjchem-29 111 20 , , PUNCT eurjchem-29 111 21     SPACE eurjchem-29 111 22 ( ( PUNCT eurjchem-29 111 23 cm‐1 cm‐1 NOUN eurjchem-29 111 24 ): ): PUNCT eurjchem-29 111 25     SPACE eurjchem-29 111 26 3212 3212 NUM eurjchem-29 111 27 , , PUNCT eurjchem-29 111 28     SPACE eurjchem-29 111 29 3209 3209 NUM eurjchem-29 111 30 , , PUNCT eurjchem-29 111 31     SPACE eurjchem-29 111 32 3184 3184 NUM eurjchem-29 111 33     SPACE eurjchem-29 111 34 ( ( PUNCT eurjchem-29 111 35 3 3 NUM eurjchem-29 111 36     SPACE eurjchem-29 111 37 nh nh NOUN eurjchem-29 111 38 ) ) PUNCT eurjchem-29 111 39 , , PUNCT eurjchem-29 111 40     SPACE eurjchem-29 111 41 2945 2945 NUM eurjchem-29 111 42     SPACE eurjchem-29 111 43 ( ( PUNCT eurjchem-29 111 44 ch2 ch2 PROPN eurjchem-29 111 45 ) ) PUNCT eurjchem-29 111 46 , , PUNCT eurjchem-29 111 47     SPACE eurjchem-29 111 48 2216 2216 NUM eurjchem-29 111 49     SPACE eurjchem-29 111 50 ( ( PUNCT eurjchem-29 111 51 c≡n c≡n PROPN eurjchem-29 111 52 ) ) PUNCT eurjchem-29 111 53 , , PUNCT eurjchem-29 111 54     SPACE eurjchem-29 111 55 1674 1674 NUM eurjchem-29 111 56     SPACE eurjchem-29 111 57 ( ( PUNCT eurjchem-29 111 58 c c NOUN eurjchem-29 111 59 = = NOUN eurjchem-29 111 60 o o NOUN eurjchem-29 111 61 ) ) PUNCT eurjchem-29 111 62 , , PUNCT eurjchem-29 111 63     SPACE eurjchem-29 111 64 1565 1565 NUM eurjchem-29 111 65     SPACE eurjchem-29 111 66 ( ( PUNCT eurjchem-29 111 67 c c NOUN eurjchem-29 111 68 = = SYM eurjchem-29 111 69 n n NUM eurjchem-29 111 70 ) ) PUNCT eurjchem-29 111 71 , , PUNCT eurjchem-29 111 72     SPACE eurjchem-29 111 73 1285 1285 NUM eurjchem-29 111 74     SPACE eurjchem-29 111 75 ( ( PUNCT eurjchem-29 111 76 c c NOUN eurjchem-29 111 77 = = SYM eurjchem-29 111 78 s s NOUN eurjchem-29 111 79 ) ) PUNCT eurjchem-29 111 80 , , PUNCT eurjchem-29 111 81     SPACE eurjchem-29 111 82 768 768 NUM eurjchem-29 111 83     SPACE eurjchem-29 111 84 ( ( PUNCT eurjchem-29 111 85 c c NOUN eurjchem-29 111 86 – – PUNCT eurjchem-29 111 87 cl cl NOUN eurjchem-29 111 88 ) ) PUNCT eurjchem-29 111 89 . . PUNCT eurjchem-29 111 90     SPACE eurjchem-29 111 91 1h 1h NUM eurjchem-29 111 92     SPACE eurjchem-29 111 93 nmr nmr NOUN eurjchem-29 111 94     SPACE eurjchem-29 111 95 ( ( PUNCT eurjchem-29 111 96 200 200 NUM eurjchem-29 111 97     SPACE eurjchem-29 111 98 mhz mhz NOUN eurjchem-29 111 99 , , PUNCT eurjchem-29 111 100     SPACE eurjchem-29 111 101 dmso‐d6 dmso‐d6 NOUN eurjchem-29 111 102 ) ) PUNCT eurjchem-29 111 103 , , PUNCT eurjchem-29 111 104     SPACE eurjchem-29 111 105 δ δ PROPN eurjchem-29 111 106 : : PUNCT eurjchem-29 111 107     SPACE eurjchem-29 111 108 4.12 4.12 NUM eurjchem-29 111 109     SPACE eurjchem-29 111 110 ( ( PUNCT eurjchem-29 111 111 s s PROPN eurjchem-29 111 112 , , PUNCT eurjchem-29 111 113     SPACE eurjchem-29 111 114 2h 2h NUM eurjchem-29 111 115 , , PUNCT eurjchem-29 111 116     SPACE eurjchem-29 111 117 ch2 ch2 NOUN eurjchem-29 111 118 ) ) PUNCT eurjchem-29 111 119 , , PUNCT eurjchem-29 111 120     SPACE eurjchem-29 111 121 7.26–8.38 7.26–8.38 NUM eurjchem-29 111 122     SPACE eurjchem-29 111 123 ( ( PUNCT eurjchem-29 111 124 m m PROPN eurjchem-29 111 125 , , PUNCT eurjchem-29 111 126     SPACE eurjchem-29 111 127 20h 20h NOUN eurjchem-29 111 128 , , PUNCT eurjchem-29 111 129     SPACE eurjchem-29 111 130 ar‐h ar‐h NOUN eurjchem-29 111 131 ) ) PUNCT eurjchem-29 111 132 , , PUNCT eurjchem-29 111 133     SPACE eurjchem-29 111 134 8.96 8.96 NUM eurjchem-29 111 135     SPACE eurjchem-29 111 136 ( ( PUNCT eurjchem-29 111 137 s s PROPN eurjchem-29 111 138 , , PUNCT eurjchem-29 111 139     SPACE eurjchem-29 111 140 1h 1h NUM eurjchem-29 111 141 , , PUNCT eurjchem-29 111 142     SPACE eurjchem-29 111 143 nh nh PROPN eurjchem-29 111 144 ) ) PUNCT eurjchem-29 111 145 , , PUNCT eurjchem-29 111 146     SPACE eurjchem-29 111 147 9.57 9.57 NUM eurjchem-29 111 148     SPACE eurjchem-29 111 149 ( ( PUNCT eurjchem-29 111 150 s s PROPN eurjchem-29 111 151 , , PUNCT eurjchem-29 111 152     SPACE eurjchem-29 111 153 1h 1h NUM eurjchem-29 111 154 , , PUNCT eurjchem-29 111 155     SPACE eurjchem-29 111 156 nh nh PROPN eurjchem-29 111 157 ) ) PUNCT eurjchem-29 111 158 , , PUNCT eurjchem-29 111 159     SPACE eurjchem-29 111 160 9.89 9.89 NUM eurjchem-29 111 161     SPACE eurjchem-29 111 162 ( ( PUNCT eurjchem-29 111 163 s s PROPN eurjchem-29 111 164 , , PUNCT eurjchem-29 111 165     SPACE eurjchem-29 111 166 1h 1h NUM eurjchem-29 111 167 , , PUNCT eurjchem-29 111 168     SPACE eurjchem-29 111 169 nh nh PROPN eurjchem-29 111 170 ) ) PUNCT eurjchem-29 111 171 . . PUNCT eurjchem-29 111 172     SPACE eurjchem-29 112 1 ms ms PROPN eurjchem-29 112 2 , , PUNCT eurjchem-29 112 3     SPACE eurjchem-29 112 4 m m PROPN eurjchem-29 112 5 / / PROPN eurjchem-29 112 6 z z NOUN eurjchem-29 112 7     SPACE eurjchem-29 112 8 ( ( PUNCT eurjchem-29 112 9 i i PRON eurjchem-29 112 10     SPACE eurjchem-29 112 11 % % INTJ eurjchem-29 112 12 ): ): PUNCT eurjchem-29 112 13     SPACE eurjchem-29 112 14 699.5 699.5 NUM eurjchem-29 112 15     SPACE eurjchem-29 112 16 ( ( PUNCT eurjchem-29 112 17 m+ m+ NUM eurjchem-29 112 18 , , PUNCT eurjchem-29 112 19     SPACE eurjchem-29 112 20 3 3 NUM eurjchem-29 112 21 % % NOUN eurjchem-29 112 22 ) ) PUNCT eurjchem-29 112 23 , , PUNCT eurjchem-29 112 24     SPACE eurjchem-29 112 25 570 570 NUM eurjchem-29 112 26     SPACE eurjchem-29 112 27 ( ( PUNCT eurjchem-29 112 28 13 13 NUM eurjchem-29 112 29 ) ) PUNCT eurjchem-29 112 30 , , PUNCT eurjchem-29 112 31     SPACE eurjchem-29 112 32 119 119 NUM eurjchem-29 112 33     SPACE eurjchem-29 112 34 ( ( PUNCT eurjchem-29 112 35 4 4 NUM eurjchem-29 112 36 ) ) PUNCT eurjchem-29 112 37 , , PUNCT eurjchem-29 112 38     SPACE eurjchem-29 112 39 114 114 NUM eurjchem-29 112 40     SPACE eurjchem-29 112 41 ( ( PUNCT eurjchem-29 112 42 3 3 NUM eurjchem-29 112 43 ) ) PUNCT eurjchem-29 112 44 , , PUNCT eurjchem-29 112 45     SPACE eurjchem-29 112 46 105 105 NUM eurjchem-29 112 47     SPACE eurjchem-29 112 48 ( ( PUNCT eurjchem-29 112 49 100 100 NUM eurjchem-29 112 50 ) ) PUNCT eurjchem-29 112 51 , , PUNCT eurjchem-29 112 52     SPACE eurjchem-29 112 53 70 70 NUM eurjchem-29 112 54     SPACE eurjchem-29 112 55 ( ( PUNCT eurjchem-29 112 56 13 13 NUM eurjchem-29 112 57 ) ) PUNCT eurjchem-29 112 58 , , PUNCT eurjchem-29 112 59     SPACE eurjchem-29 112 60 41 41 NUM eurjchem-29 112 61     SPACE eurjchem-29 112 62 ( ( PUNCT eurjchem-29 112 63 17 17 NUM eurjchem-29 112 64 ) ) PUNCT eurjchem-29 112 65 . . PUNCT eurjchem-29 112 66     SPACE eurjchem-29 113 1 anal anal ADJ eurjchem-29 113 2 . . PUNCT eurjchem-29 113 3     SPACE eurjchem-29 113 4 calcd calcd NOUN eurjchem-29 113 5 . . PUNCT eurjchem-29 113 6     SPACE eurjchem-29 113 7 for for ADP eurjchem-29 113 8     SPACE eurjchem-29 113 9 c34h22n11os2cl c34h22n11os2cl PROPN eurjchem-29 113 10     SPACE eurjchem-29 113 11 ( ( PUNCT eurjchem-29 113 12 699.5 699.5 NUM eurjchem-29 113 13 ): ): SYM eurjchem-29 113 14     SPACE eurjchem-29 113 15 c c NOUN eurjchem-29 113 16 , , PUNCT eurjchem-29 113 17     SPACE eurjchem-29 113 18 58.32 58.32 NUM eurjchem-29 113 19 ; ; PUNCT eurjchem-29 113 20     SPACE eurjchem-29 113 21 h h NOUN eurjchem-29 113 22 , , PUNCT eurjchem-29 113 23     SPACE eurjchem-29 113 24 3.14 3.14 NUM eurjchem-29 113 25 ; ; PUNCT eurjchem-29 113 26     SPACE eurjchem-29 113 27 n n CCONJ eurjchem-29 113 28 , , PUNCT eurjchem-29 113 29     SPACE eurjchem-29 113 30 22.01 22.01 NUM eurjchem-29 113 31 ; ; PUNCT eurjchem-29 113 32     SPACE eurjchem-29 113 33 s s PROPN eurjchem-29 113 34 , , PUNCT eurjchem-29 113 35     SPACE eurjchem-29 113 36 9.14 9.14 NUM eurjchem-29 113 37     SPACE eurjchem-29 113 38 cl cl NOUN eurjchem-29 113 39 , , PUNCT eurjchem-29 113 40     SPACE eurjchem-29 113 41 5.07 5.07 NUM eurjchem-29 113 42 . . PUNCT eurjchem-29 113 43     SPACE eurjchem-29 113 44 found find VERB eurjchem-29 113 45 : : PUNCT eurjchem-29 113 46     SPACE eurjchem-29 113 47 c c X eurjchem-29 113 48 , , PUNCT eurjchem-29 113 49     SPACE eurjchem-29 113 50 58.66 58.66 NUM eurjchem-29 113 51 ; ; PUNCT eurjchem-29 113 52     SPACE eurjchem-29 113 53 h h NOUN eurjchem-29 113 54 , , PUNCT eurjchem-29 113 55     SPACE eurjchem-29 113 56 3.43 3.43 NUM eurjchem-29 113 57 ; ; PUNCT eurjchem-29 113 58     SPACE eurjchem-29 113 59 n n CCONJ eurjchem-29 113 60 , , PUNCT eurjchem-29 113 61     SPACE eurjchem-29 113 62 22.35 22.35 NUM eurjchem-29 113 63 ; ; PUNCT eurjchem-29 113 64     SPACE eurjchem-29 113 65 s s PROPN eurjchem-29 113 66 , , PUNCT eurjchem-29 113 67     SPACE eurjchem-29 113 68 9.35 9.35 NUM eurjchem-29 113 69 ; ; PUNCT eurjchem-29 113 70     SPACE eurjchem-29 113 71 cl cl NOUN eurjchem-29 113 72 , , PUNCT eurjchem-29 113 73     SPACE eurjchem-29 113 74 5.31 5.31 NUM eurjchem-29 113 75 % % NOUN eurjchem-29 113 76 . . PUNCT eurjchem-29 113 77           SPACE eurjchem-29 114 1 2.3 2.3 NUM eurjchem-29 114 2 . . PUNCT eurjchem-29 114 3     SPACE eurjchem-29 114 4 antimicrobial antimicrobial ADJ eurjchem-29 114 5     SPACE eurjchem-29 114 6 screening screening NOUN eurjchem-29 114 7         SPACE eurjchem-29 114 8 representative representative NOUN eurjchem-29 114 9     SPACE eurjchem-29 114 10 compounds compound NOUN eurjchem-29 114 11     SPACE eurjchem-29 114 12 of of ADP eurjchem-29 114 13     SPACE eurjchem-29 114 14 the the DET eurjchem-29 114 15     SPACE eurjchem-29 114 16 synthesized synthesize VERB eurjchem-29 114 17     SPACE eurjchem-29 114 18 products product NOUN eurjchem-29 114 19     SPACE eurjchem-29 114 20 were be AUX eurjchem-29 114 21     SPACE eurjchem-29 114 22 screened screen VERB eurjchem-29 114 23     SPACE eurjchem-29 114 24 in in ADP eurjchem-29 114 25     SPACE eurjchem-29 114 26 vitro vitro X eurjchem-29 114 27     SPACE eurjchem-29 114 28 for for ADP eurjchem-29 114 29     SPACE eurjchem-29 114 30 their their PRON eurjchem-29 114 31     SPACE eurjchem-29 114 32 antimicrobial antimicrobial ADJ eurjchem-29 114 33     SPACE eurjchem-29 114 34 activities activity NOUN eurjchem-29 114 35     SPACE eurjchem-29 114 36 against against ADP eurjchem-29 114 37     SPACE eurjchem-29 114 38 two two NUM eurjchem-29 114 39     SPACE eurjchem-29 114 40 strains strain NOUN eurjchem-29 114 41     SPACE eurjchem-29 114 42 of of ADP eurjchem-29 114 43     SPACE eurjchem-29 114 44 bacteria bacteria NOUN eurjchem-29 114 45     SPACE eurjchem-29 114 46 bacillus bacillus NOUN eurjchem-29 114 47     SPACE eurjchem-29 114 48 subtilis subtili NOUN eurjchem-29 114 49     SPACE eurjchem-29 114 50 and and CCONJ eurjchem-29 114 51     SPACE eurjchem-29 114 52 escherichia escherichia NOUN eurjchem-29 114 53     SPACE eurjchem-29 114 54 coli coli NOUN eurjchem-29 114 55     SPACE eurjchem-29 114 56 and and CCONJ eurjchem-29 114 57     SPACE eurjchem-29 114 58 two two NUM eurjchem-29 114 59     SPACE eurjchem-29 114 60 strains strain NOUN eurjchem-29 114 61     SPACE eurjchem-29 114 62 of of ADP eurjchem-29 114 63     SPACE eurjchem-29 114 64 fungi fungi PROPN eurjchem-29 114 65     SPACE eurjchem-29 114 66 aspergillus aspergillus NOUN eurjchem-29 114 67     SPACE eurjchem-29 114 68 fumigatus fumigatus NOUN eurjchem-29 114 69     SPACE eurjchem-29 114 70 and and CCONJ eurjchem-29 114 71     SPACE eurjchem-29 114 72 candida candida NOUN eurjchem-29 114 73     SPACE eurjchem-29 114 74 albicans albican NOUN eurjchem-29 114 75     SPACE eurjchem-29 114 76 by by ADP eurjchem-29 114 77     SPACE eurjchem-29 114 78 the the DET eurjchem-29 114 79     SPACE eurjchem-29 114 80 agar agar NOUN eurjchem-29 114 81     SPACE eurjchem-29 114 82 diffusion diffusion NOUN eurjchem-29 114 83     SPACE eurjchem-29 114 84 method method NOUN eurjchem-29 114 85     SPACE eurjchem-29 114 86 [ [ X eurjchem-29 114 87 21–23 21–23 NUM eurjchem-29 114 88 ] ] X eurjchem-29 114 89 . . PUNCT eurjchem-29 114 90     SPACE eurjchem-29 115 1 the the DET eurjchem-29 115 2     SPACE eurjchem-29 115 3 dishes dish NOUN eurjchem-29 115 4     SPACE eurjchem-29 115 5 were be AUX eurjchem-29 115 6     SPACE eurjchem-29 115 7 incubated incubate VERB eurjchem-29 115 8     SPACE eurjchem-29 115 9 at at ADP eurjchem-29 115 10     SPACE eurjchem-29 115 11 37 37 NUM eurjchem-29 115 12     SPACE eurjchem-29 115 13 ºc ºc NOUN eurjchem-29 115 14     SPACE eurjchem-29 115 15 for for ADP eurjchem-29 115 16     SPACE eurjchem-29 115 17 48 48 NUM eurjchem-29 115 18     SPACE eurjchem-29 115 19 hr hr NOUN eurjchem-29 115 20     SPACE eurjchem-29 115 21 ( ( PUNCT eurjchem-29 115 22 for for ADP eurjchem-29 115 23     SPACE eurjchem-29 115 24 bacteria bacteria NOUN eurjchem-29 115 25 ) ) PUNCT eurjchem-29 115 26     SPACE eurjchem-29 115 27 and and CCONJ eurjchem-29 115 28     SPACE eurjchem-29 115 29 at at ADP eurjchem-29 115 30     SPACE eurjchem-29 115 31 30 30 NUM eurjchem-29 115 32     SPACE eurjchem-29 115 33 ºc ºc NOUN eurjchem-29 115 34     SPACE eurjchem-29 115 35 for for ADP eurjchem-29 115 36     SPACE eurjchem-29 115 37 72 72 NUM eurjchem-29 115 38     SPACE eurjchem-29 115 39 hr hr NOUN eurjchem-29 115 40     SPACE eurjchem-29 115 41 ( ( PUNCT eurjchem-29 115 42 for for ADP eurjchem-29 115 43     SPACE eurjchem-29 115 44 fungi fungus NOUN eurjchem-29 115 45 ) ) PUNCT eurjchem-29 115 46 , , PUNCT eurjchem-29 115 47     SPACE eurjchem-29 115 48 where where SCONJ eurjchem-29 115 49     SPACE eurjchem-29 115 50 clear clear ADJ eurjchem-29 115 51     SPACE eurjchem-29 115 52 or or CCONJ eurjchem-29 115 53     SPACE eurjchem-29 115 54 inhibition inhibition NOUN eurjchem-29 115 55     SPACE eurjchem-29 115 56 zones zone NOUN eurjchem-29 115 57     SPACE eurjchem-29 115 58 were be AUX eurjchem-29 115 59     SPACE eurjchem-29 115 60 detected detect VERB eurjchem-29 115 61     SPACE eurjchem-29 115 62 around around ADP eurjchem-29 115 63     SPACE eurjchem-29 115 64 each each DET eurjchem-29 115 65     SPACE eurjchem-29 115 66 hole hole NOUN eurjchem-29 115 67 . . PUNCT eurjchem-29 115 68     SPACE eurjchem-29 116 1 each each DET eurjchem-29 116 2     SPACE eurjchem-29 116 3 0.1 0.1 NUM eurjchem-29 116 4     SPACE eurjchem-29 116 5 ml ml NOUN eurjchem-29 116 6     SPACE eurjchem-29 116 7 of of ADP eurjchem-29 116 8     SPACE eurjchem-29 116 9 dmf dmf PROPN eurjchem-29 116 10     SPACE eurjchem-29 116 11 alone alone ADV eurjchem-29 116 12     SPACE eurjchem-29 116 13 was be AUX eurjchem-29 116 14     SPACE eurjchem-29 116 15 used use VERB eurjchem-29 116 16     SPACE eurjchem-29 116 17 as as ADP eurjchem-29 116 18     SPACE eurjchem-29 116 19 a a DET eurjchem-29 116 20     SPACE eurjchem-29 116 21 control control NOUN eurjchem-29 116 22     SPACE eurjchem-29 116 23 under under ADP eurjchem-29 116 24     SPACE eurjchem-29 116 25 the the DET eurjchem-29 116 26     SPACE eurjchem-29 116 27 same same ADJ eurjchem-29 116 28     SPACE eurjchem-29 116 29 conditions condition NOUN eurjchem-29 116 30     SPACE eurjchem-29 116 31 for for ADP eurjchem-29 116 32     SPACE eurjchem-29 116 33 each each DET eurjchem-29 116 34     SPACE eurjchem-29 116 35 microorganism microorganism NOUN eurjchem-29 116 36     SPACE eurjchem-29 116 37 and and CCONJ eurjchem-29 116 38     SPACE eurjchem-29 116 39 by by ADP eurjchem-29 116 40     SPACE eurjchem-29 116 41 subtracting subtract VERB eurjchem-29 116 42     SPACE eurjchem-29 116 43 the the DET eurjchem-29 116 44     SPACE eurjchem-29 116 45 diameter diameter NOUN eurjchem-29 116 46     SPACE eurjchem-29 116 47 of of ADP eurjchem-29 116 48     SPACE eurjchem-29 116 49 inhibition inhibition NOUN eurjchem-29 116 50     SPACE eurjchem-29 116 51 zone zone NOUN eurjchem-29 116 52     SPACE eurjchem-29 116 53 resulting result VERB eurjchem-29 116 54     SPACE eurjchem-29 116 55 with with ADP eurjchem-29 116 56     SPACE eurjchem-29 116 57 dmf dmf PROPN eurjchem-29 116 58     SPACE eurjchem-29 116 59 alone alone ADV eurjchem-29 116 60     SPACE eurjchem-29 116 61 from from ADP eurjchem-29 116 62     SPACE eurjchem-29 116 63 that that PRON eurjchem-29 116 64     SPACE eurjchem-29 116 65 obtained obtain VERB eurjchem-29 116 66     SPACE eurjchem-29 116 67 from from ADP eurjchem-29 116 68     SPACE eurjchem-29 116 69 that that PRON eurjchem-29 116 70     SPACE eurjchem-29 116 71 obtained obtain VERB eurjchem-29 116 72     SPACE eurjchem-29 116 73 in in ADP eurjchem-29 116 74     SPACE eurjchem-29 116 75 each each DET eurjchem-29 116 76     SPACE eurjchem-29 116 77 case case NOUN eurjchem-29 116 78     SPACE eurjchem-29 116 79 as as ADP eurjchem-29 116 80     SPACE eurjchem-29 116 81 a a DET eurjchem-29 116 82     SPACE eurjchem-29 116 83 mean mean NOUN eurjchem-29 116 84     SPACE eurjchem-29 116 85 of of ADP eurjchem-29 116 86     SPACE eurjchem-29 116 87 three three NUM eurjchem-29 116 88     SPACE eurjchem-29 116 89 replicates replicate NOUN eurjchem-29 116 90     SPACE eurjchem-29 116 91 ( ( PUNCT eurjchem-29 116 92 table table NOUN eurjchem-29 116 93     SPACE eurjchem-29 116 94 1 1 NUM eurjchem-29 116 95 ) ) PUNCT eurjchem-29 116 96 . . PUNCT eurjchem-29 116 97     SPACE eurjchem-29 117 1 terbinafin terbinafin NOUN eurjchem-29 117 2     SPACE eurjchem-29 117 3 used use VERB eurjchem-29 117 4     SPACE eurjchem-29 117 5 as as ADP eurjchem-29 117 6     SPACE eurjchem-29 117 7 a a DET eurjchem-29 117 8     SPACE eurjchem-29 117 9 standard standard ADJ eurjchem-29 117 10     SPACE eurjchem-29 117 11 antifungal antifungal ADJ eurjchem-29 117 12     SPACE eurjchem-29 117 13 agent agent NOUN eurjchem-29 117 14     SPACE eurjchem-29 117 15 and and CCONJ eurjchem-29 117 16     SPACE eurjchem-29 117 17 chloramphenicol chloramphenicol NOUN eurjchem-29 117 18     SPACE eurjchem-29 117 19 used use VERB eurjchem-29 117 20     SPACE eurjchem-29 117 21 as as ADP eurjchem-29 117 22     SPACE eurjchem-29 117 23 a a DET eurjchem-29 117 24     SPACE eurjchem-29 117 25 standard standard ADJ eurjchem-29 117 26     SPACE eurjchem-29 117 27 antibacterial antibacterial ADJ eurjchem-29 117 28     SPACE eurjchem-29 117 29 agent agent NOUN eurjchem-29 117 30 . . PUNCT eurjchem-29 117 31         SPACE eurjchem-29 118 1 3 3 NUM eurjchem-29 118 2 . . PUNCT eurjchem-29 118 3     SPACE eurjchem-29 118 4 results result VERB eurjchem-29 118 5     SPACE eurjchem-29 118 6 and and CCONJ eurjchem-29 118 7     SPACE eurjchem-29 118 8 discussion discussion NOUN eurjchem-29 118 9           SPACE eurjchem-29 118 10 3.1 3.1 NUM eurjchem-29 118 11 . . PUNCT eurjchem-29 118 12     SPACE eurjchem-29 118 13 synthesis synthesis NOUN eurjchem-29 118 14         SPACE eurjchem-29 118 15 the the DET eurjchem-29 118 16     SPACE eurjchem-29 118 17 reaction reaction NOUN eurjchem-29 118 18     SPACE eurjchem-29 118 19 of of ADP eurjchem-29 118 20     SPACE eurjchem-29 118 21 ethyl ethyl PROPN eurjchem-29 118 22     SPACE eurjchem-29 118 23 1,2‐diamino‐5‐cyano‐4‐(4‐chloro/3‐ 1,2‐diamino‐5‐cyano‐4‐(4‐chloro/3‐ NOUN eurjchem-29 118 24 nitrophenyl)‐6‐oxo‐1,6‐dihydropyridine‐3‐carboxylate nitrophenyl)‐6‐oxo‐1,6‐dihydropyridine‐3‐carboxylate NUM eurjchem-29 118 25     SPACE eurjchem-29 118 26 ( ( PUNCT eurjchem-29 118 27 2a 2a NUM eurjchem-29 118 28 , , PUNCT eurjchem-29 118 29 b b NOUN eurjchem-29 118 30 ) ) PUNCT eurjchem-29 118 31     SPACE eurjchem-29 118 32 with with SCONJ eurjchem-29 118 33     SPACE eurjchem-29 118 34 triethylorthoformate triethylorthoformate NOUN eurjchem-29 118 35     SPACE eurjchem-29 118 36 followed follow VERB eurjchem-29 118 37     SPACE eurjchem-29 118 38 by by ADP eurjchem-29 118 39     SPACE eurjchem-29 118 40 hydrazinolysis hydrazinolysis NOUN eurjchem-29 118 41     SPACE eurjchem-29 118 42 of of ADP eurjchem-29 118 43     SPACE eurjchem-29 118 44 compound compound NOUN eurjchem-29 118 45     SPACE eurjchem-29 118 46 3a 3a NUM eurjchem-29 118 47 , , PUNCT eurjchem-29 118 48     SPACE eurjchem-29 118 49 b b NOUN eurjchem-29 118 50     SPACE eurjchem-29 118 51 in in ADP eurjchem-29 118 52     SPACE eurjchem-29 118 53 boiling boil VERB eurjchem-29 118 54     SPACE eurjchem-29 118 55 ethanol ethanol NOUN eurjchem-29 118 56     SPACE eurjchem-29 118 57 afforded afford VERB eurjchem-29 118 58     SPACE eurjchem-29 118 59 the the DET eurjchem-29 118 60     SPACE eurjchem-29 118 61 corresponding corresponding ADJ eurjchem-29 118 62     SPACE eurjchem-29 118 63 carbohydrazide carbohydrazide NOUN eurjchem-29 118 64     SPACE eurjchem-29 118 65 derivatives derivative NOUN eurjchem-29 118 66     SPACE eurjchem-29 118 67 4a 4a NOUN eurjchem-29 118 68 , , PUNCT eurjchem-29 118 69 b b NOUN eurjchem-29 118 70     SPACE eurjchem-29 118 71 ( ( PUNCT eurjchem-29 118 72 scheme scheme NOUN eurjchem-29 118 73     SPACE eurjchem-29 118 74 1 1 NUM eurjchem-29 118 75 ) ) PUNCT eurjchem-29 118 76 . . PUNCT eurjchem-29 118 77     SPACE eurjchem-29 119 1 cycloconden‐ cycloconden‐ NOUN eurjchem-29 119 2 sation sation NOUN eurjchem-29 119 3     SPACE eurjchem-29 119 4 of of ADP eurjchem-29 119 5     SPACE eurjchem-29 119 6 4a 4a NOUN eurjchem-29 119 7 , , PUNCT eurjchem-29 119 8     SPACE eurjchem-29 119 9 b b NOUN eurjchem-29 119 10     SPACE eurjchem-29 119 11 with with ADP eurjchem-29 119 12     SPACE eurjchem-29 119 13 2‐hydroxy‐1,2‐diphenylethanone 2‐hydroxy‐1,2‐diphenylethanone NOUN eurjchem-29 119 14     SPACE eurjchem-29 119 15 in in ADP eurjchem-29 119 16     SPACE eurjchem-29 119 17 dmf dmf PROPN eurjchem-29 119 18     SPACE eurjchem-29 119 19 afforded afford VERB eurjchem-29 119 20     SPACE eurjchem-29 119 21 the the DET eurjchem-29 119 22     SPACE eurjchem-29 119 23 required require VERB eurjchem-29 119 24     SPACE eurjchem-29 119 25 starting starting NOUN eurjchem-29 119 26     SPACE eurjchem-29 119 27 compounds compound VERB eurjchem-29 119 28     SPACE eurjchem-29 119 29 7‐aryl 7‐aryl NUM eurjchem-29 119 30     SPACE eurjchem-29 119 31 8‐ 8‐ NUM eurjchem-29 119 32 oxadiazinyltriazolopyridine oxadiazinyltriazolopyridine NOUN eurjchem-29 119 33     SPACE eurjchem-29 119 34 derivatives derivative NOUN eurjchem-29 119 35     SPACE eurjchem-29 119 36 5a 5a NUM eurjchem-29 119 37 , , PUNCT eurjchem-29 119 38 b. b. PROPN eurjchem-29 119 39     SPACE eurjchem-29 119 40 structures structure NOUN eurjchem-29 119 41     SPACE eurjchem-29 119 42 of of ADP eurjchem-29 119 43     SPACE eurjchem-29 119 44 the the DET eurjchem-29 119 45     SPACE eurjchem-29 119 46 compounds compound NOUN eurjchem-29 119 47     SPACE eurjchem-29 119 48 5a 5a NUM eurjchem-29 119 49 , , PUNCT eurjchem-29 119 50 b b AUX eurjchem-29 119 51     SPACE eurjchem-29 119 52 were be AUX eurjchem-29 119 53     SPACE eurjchem-29 119 54 based base VERB eurjchem-29 119 55     SPACE eurjchem-29 119 56 on on ADP eurjchem-29 119 57     SPACE eurjchem-29 119 58 analytical analytical ADJ eurjchem-29 119 59     SPACE eurjchem-29 119 60 and and CCONJ eurjchem-29 119 61     SPACE eurjchem-29 119 62 spectral spectral ADJ eurjchem-29 119 63     SPACE eurjchem-29 119 64 data datum NOUN eurjchem-29 119 65 . . PUNCT eurjchem-29 119 66     SPACE eurjchem-29 120 1 the the DET eurjchem-29 120 2     SPACE eurjchem-29 120 3 1h 1h NUM eurjchem-29 120 4     SPACE eurjchem-29 120 5 nmr nmr NOUN eurjchem-29 120 6     SPACE eurjchem-29 120 7 spectrum spectrum NOUN eurjchem-29 120 8     SPACE eurjchem-29 120 9 of of ADP eurjchem-29 120 10     SPACE eurjchem-29 120 11 5a 5a NUM eurjchem-29 120 12     SPACE eurjchem-29 120 13 revealed reveal VERB eurjchem-29 120 14     SPACE eurjchem-29 120 15 the the DET eurjchem-29 120 16     SPACE eurjchem-29 120 17 appearance appearance NOUN eurjchem-29 120 18     SPACE eurjchem-29 120 19 of of ADP eurjchem-29 120 20     SPACE eurjchem-29 120 21 characteristic characteristic ADJ eurjchem-29 120 22     SPACE eurjchem-29 120 23 singlet singlet NOUN eurjchem-29 120 24     SPACE eurjchem-29 120 25 at at ADP eurjchem-29 120 26     SPACE eurjchem-29 120 27 δ δ PROPN eurjchem-29 120 28     SPACE eurjchem-29 120 29 5.71 5.71 NUM eurjchem-29 120 30     SPACE eurjchem-29 120 31 and and CCONJ eurjchem-29 120 32     SPACE eurjchem-29 120 33 8.77 8.77 NUM eurjchem-29 120 34     SPACE eurjchem-29 120 35 ppm ppm NOUN eurjchem-29 120 36     SPACE eurjchem-29 120 37 assigned assign VERB eurjchem-29 120 38     SPACE eurjchem-29 120 39 to to ADP eurjchem-29 120 40     SPACE eurjchem-29 120 41 nh nh NOUN eurjchem-29 120 42     SPACE eurjchem-29 120 43 protons proton NOUN eurjchem-29 120 44     SPACE eurjchem-29 120 45 of of ADP eurjchem-29 120 46     SPACE eurjchem-29 120 47 1,3,4‐oxadiazione 1,3,4‐oxadiazione NUM eurjchem-29 120 48     SPACE eurjchem-29 120 49 moieties moiety NOUN eurjchem-29 120 50 . . PUNCT eurjchem-29 120 51     SPACE eurjchem-29 121 1 the the DET eurjchem-29 121 2     SPACE eurjchem-29 121 3 compounds compound VERB eurjchem-29 121 4     SPACE eurjchem-29 121 5 5a 5a NUM eurjchem-29 121 6 , , PUNCT eurjchem-29 121 7     SPACE eurjchem-29 121 8 b b NOUN eurjchem-29 121 9     SPACE eurjchem-29 121 10 were be AUX eurjchem-29 121 11     SPACE eurjchem-29 121 12 used use VERB eurjchem-29 121 13     SPACE eurjchem-29 121 14 for for ADP eurjchem-29 121 15     SPACE eurjchem-29 121 16 the the DET eurjchem-29 121 17     SPACE eurjchem-29 121 18 synthesis synthesis NOUN eurjchem-29 121 19     SPACE eurjchem-29 121 20 of of ADP eurjchem-29 121 21     SPACE eurjchem-29 121 22 1,2,4‐ 1,2,4‐ NUM eurjchem-29 121 23 triazine triazine NOUN eurjchem-29 121 24     SPACE eurjchem-29 121 25 systems system NOUN eurjchem-29 121 26 . . PUNCT eurjchem-29 121 27     SPACE eurjchem-29 122 1 thus thus ADV eurjchem-29 122 2 , , PUNCT eurjchem-29 122 3     SPACE eurjchem-29 122 4 cyclocondensation cyclocondensation NOUN eurjchem-29 122 5     SPACE eurjchem-29 122 6 of of ADP eurjchem-29 122 7     SPACE eurjchem-29 122 8 5a 5a NUM eurjchem-29 122 9 , , PUNCT eurjchem-29 122 10 b b NOUN eurjchem-29 122 11     SPACE eurjchem-29 122 12 with with ADP eurjchem-29 122 13     SPACE eurjchem-29 122 14 2‐ 2‐ NUM eurjchem-29 122 15 amino‐1,3‐thiazole amino‐1,3‐thiazole PROPN eurjchem-29 122 16     SPACE eurjchem-29 122 17 in in ADP eurjchem-29 122 18     SPACE eurjchem-29 122 19 dry dry ADJ eurjchem-29 122 20     SPACE eurjchem-29 122 21 pyridine pyridine NOUN eurjchem-29 122 22     SPACE eurjchem-29 123 1 [ [ X eurjchem-29 123 2 24 24 NUM eurjchem-29 123 3 ] ] PUNCT eurjchem-29 123 4     SPACE eurjchem-29 123 5 gave give VERB eurjchem-29 123 6     SPACE eurjchem-29 123 7 7‐(4‐chloro/3‐ 7‐(4‐chloro/3‐ NUM eurjchem-29 123 8 nitrophenyl)‐8‐[5,6‐diphenyl‐4‐(1,3‐thiazol‐2‐yl)‐1,4‐dihydro‐ nitrophenyl)‐8‐[5,6‐diphenyl‐4‐(1,3‐thiazol‐2‐yl)‐1,4‐dihydro‐ NOUN eurjchem-29 123 9 1,2,4‐triazin‐3‐yl]‐5‐oxo‐1,5‐dihydro[1,2,4]triazolo[1,5‐a]pyri 1,2,4‐triazin‐3‐yl]‐5‐oxo‐1,5‐dihydro[1,2,4]triazolo[1,5‐a]pyri NUM eurjchem-29 123 10     SPACE eurjchem-29 123 11 dine‐6‐carbonitrile dine‐6‐carbonitrile NOUN eurjchem-29 123 12     SPACE eurjchem-29 123 13 ( ( PUNCT eurjchem-29 123 14 6a 6a NOUN eurjchem-29 123 15 , , PUNCT eurjchem-29 123 16 b b NOUN eurjchem-29 123 17 ) ) PUNCT eurjchem-29 123 18     SPACE eurjchem-29 123 19 ( ( PUNCT eurjchem-29 123 20 scheme scheme NOUN eurjchem-29 123 21     SPACE eurjchem-29 123 22 1 1 NUM eurjchem-29 123 23 ) ) PUNCT eurjchem-29 123 24 . . PUNCT eurjchem-29 123 25     SPACE eurjchem-29 124 1 structures structure NOUN eurjchem-29 124 2     SPACE eurjchem-29 124 3 of of ADP eurjchem-29 124 4     SPACE eurjchem-29 124 5 compounds compound NOUN eurjchem-29 124 6     SPACE eurjchem-29 124 7 6a 6a NOUN eurjchem-29 124 8 , , PUNCT eurjchem-29 124 9     SPACE eurjchem-29 124 10 b b NOUN eurjchem-29 124 11     SPACE eurjchem-29 124 12 were be AUX eurjchem-29 124 13     SPACE eurjchem-29 124 14 elucidated elucidated ADJ eurjchem-29 124 15     SPACE eurjchem-29 124 16 on on ADP eurjchem-29 124 17     SPACE eurjchem-29 124 18 the the DET eurjchem-29 124 19     SPACE eurjchem-29 124 20 basis basis NOUN eurjchem-29 124 21     SPACE eurjchem-29 124 22 of of ADP eurjchem-29 124 23     SPACE eurjchem-29 124 24 elemental elemental ADJ eurjchem-29 124 25     SPACE eurjchem-29 124 26 analysis analysis NOUN eurjchem-29 124 27     SPACE eurjchem-29 124 28 and and CCONJ eurjchem-29 124 29     SPACE eurjchem-29 124 30 spectral spectral ADJ eurjchem-29 124 31     SPACE eurjchem-29 124 32 data datum NOUN eurjchem-29 124 33     SPACE eurjchem-29 124 34 ( ( PUNCT eurjchem-29 124 35 see see VERB eurjchem-29 124 36     SPACE eurjchem-29 124 37 experimental experimental ADJ eurjchem-29 124 38     SPACE eurjchem-29 124 39 section section NOUN eurjchem-29 124 40 ) ) PUNCT eurjchem-29 124 41 . . PUNCT eurjchem-29 124 42           SPACE eurjchem-29 125 1 chemical chemical NOUN eurjchem-29 125 2     SPACE eurjchem-29 125 3 reactivity reactivity NOUN eurjchem-29 125 4     SPACE eurjchem-29 125 5 of of ADP eurjchem-29 125 6     SPACE eurjchem-29 125 7 interesting interesting ADJ eurjchem-29 125 8     SPACE eurjchem-29 125 9 functionally functionally ADV eurjchem-29 125 10     SPACE eurjchem-29 125 11 substituted substitute VERB eurjchem-29 125 12     SPACE eurjchem-29 125 13 1,2,4‐triazines 1,2,4‐triazine NOUN eurjchem-29 125 14     SPACE eurjchem-29 125 15 6a 6a NOUN eurjchem-29 125 16 , , PUNCT eurjchem-29 125 17 b b X eurjchem-29 125 18     SPACE eurjchem-29 125 19 have have AUX eurjchem-29 125 20     SPACE eurjchem-29 125 21 received receive VERB eurjchem-29 125 22     SPACE eurjchem-29 125 23 considerable considerable ADJ eurjchem-29 125 24     SPACE eurjchem-29 125 25 attention attention NOUN eurjchem-29 125 26 . . PUNCT eurjchem-29 125 27     SPACE eurjchem-29 126 1 thus thus ADV eurjchem-29 126 2 , , PUNCT eurjchem-29 126 3     SPACE eurjchem-29 126 4 acylation acylation NOUN eurjchem-29 126 5     SPACE eurjchem-29 126 6 of of ADP eurjchem-29 126 7     SPACE eurjchem-29 126 8 b b NOUN eurjchem-29 126 9     SPACE eurjchem-29 126 10 using use VERB eurjchem-29 126 11     SPACE eurjchem-29 126 12 chloroacetyl chloroacetyl NOUN eurjchem-29 126 13     SPACE eurjchem-29 126 14 chloride chloride NOUN eurjchem-29 126 15     SPACE eurjchem-29 126 16 in in ADP eurjchem-29 126 17     SPACE eurjchem-29 126 18 dry dry PROPN eurjchem-29 126 19     SPACE eurjchem-29 126 20 dmf dmf PROPN eurjchem-29 126 21     SPACE eurjchem-29 126 22 afforded afford VERB eurjchem-29 126 23     SPACE eurjchem-29 126 24 8‐[5,6‐diphenyl‐4‐(1,3‐thiazol‐2‐yl)‐1h‐1,2,4‐triazin‐3‐yl]‐7‐(3‐ 8‐[5,6‐diphenyl‐4‐(1,3‐thiazol‐2‐yl)‐1h‐1,2,4‐triazin‐3‐yl]‐7‐(3‐ PROPN eurjchem-29 126 25 nitrophenyl)‐5‐oxo‐1‐(chloroacetyl)[1,2,4]triazolo[1,5‐a]pyridi nitrophenyl)‐5‐oxo‐1‐(chloroacetyl)[1,2,4]triazolo[1,5‐a]pyridi NOUN eurjchem-29 126 26     SPACE eurjchem-29 126 27 ne‐6‐carbonit‐rile ne‐6‐carbonit‐rile ADV eurjchem-29 126 28     SPACE eurjchem-29 126 29 ( ( PUNCT eurjchem-29 126 30 7 7 NUM eurjchem-29 126 31 ) ) PUNCT eurjchem-29 126 32     SPACE eurjchem-29 126 33 which which DET eurjchem-29 126 34     SPACE eurjchem-29 126 35 underwent underwent NOUN eurjchem-29 126 36     SPACE eurjchem-29 126 37 cyclocondensation cyclocondensation NOUN eurjchem-29 126 38     SPACE eurjchem-29 126 39 reaction reaction NOUN eurjchem-29 126 40     SPACE eurjchem-29 126 41 with with ADP eurjchem-29 126 42     SPACE eurjchem-29 126 43 guanidine guanidine NOUN eurjchem-29 126 44     SPACE eurjchem-29 126 45 hydrochloride hydrochloride NOUN eurjchem-29 126 46     SPACE eurjchem-29 126 47 in in ADP eurjchem-29 126 48     SPACE eurjchem-29 126 49 the the DET eurjchem-29 126 50     SPACE eurjchem-29 126 51 presence presence NOUN eurjchem-29 126 52     SPACE eurjchem-29 126 53 of of ADP eurjchem-29 126 54     SPACE eurjchem-29 126 55 dmf dmf PROPN eurjchem-29 126 56     SPACE eurjchem-29 126 57 to to PART eurjchem-29 126 58     SPACE eurjchem-29 126 59 give give VERB eurjchem-29 126 60     SPACE eurjchem-29 126 61 8‐triazinyltriazolopyridine 8‐triazinyltriazolopyridine NOUN eurjchem-29 126 62     SPACE eurjchem-29 126 63 derivative derivative NOUN eurjchem-29 126 64     SPACE eurjchem-29 126 65 8 8 NUM eurjchem-29 126 66     SPACE eurjchem-29 126 67 ( ( PUNCT eurjchem-29 126 68 scheme scheme NOUN eurjchem-29 126 69     SPACE eurjchem-29 126 70 2 2 NUM eurjchem-29 126 71 ) ) PUNCT eurjchem-29 126 72 . . PUNCT eurjchem-29 126 73     SPACE eurjchem-29 126 74 disappearance disappearance NOUN eurjchem-29 126 75     SPACE eurjchem-29 126 76 of of ADP eurjchem-29 126 77     SPACE eurjchem-29 126 78 only only ADV eurjchem-29 126 79     SPACE eurjchem-29 126 80 nh nh PROPN eurjchem-29 126 81     SPACE eurjchem-29 126 82 triazole triazole NOUN eurjchem-29 126 83     SPACE eurjchem-29 126 84 proton proton NOUN eurjchem-29 126 85     SPACE eurjchem-29 126 86 in in ADP eurjchem-29 126 87     SPACE eurjchem-29 126 88 the the DET eurjchem-29 126 89     SPACE eurjchem-29 126 90 1h 1h NUM eurjchem-29 126 91     SPACE eurjchem-29 126 92 nmr nmr NOUN eurjchem-29 126 93     SPACE eurjchem-29 126 94 spectrum spectrum NOUN eurjchem-29 126 95     SPACE eurjchem-29 126 96 of of ADP eurjchem-29 126 97     SPACE eurjchem-29 126 98 7 7 NUM eurjchem-29 126 99     SPACE eurjchem-29 126 100 supported support VERB eurjchem-29 126 101     SPACE eurjchem-29 126 102 that that SCONJ eurjchem-29 126 103     SPACE eurjchem-29 126 104 acylation acylation NOUN eurjchem-29 126 105     SPACE eurjchem-29 126 106 process process NOUN eurjchem-29 126 107     SPACE eurjchem-29 126 108 occurred occur VERB eurjchem-29 126 109     SPACE eurjchem-29 126 110 on on ADP eurjchem-29 126 111     SPACE eurjchem-29 126 112 nh nh PROPN eurjchem-29 126 113     SPACE eurjchem-29 126 114 triazole triazole NOUN eurjchem-29 126 115     SPACE eurjchem-29 126 116 and and CCONJ eurjchem-29 126 117     SPACE eurjchem-29 126 118 not not PART eurjchem-29 126 119     SPACE eurjchem-29 126 120 nh nh NOUN eurjchem-29 126 121     SPACE eurjchem-29 126 122 triazine triazine NOUN eurjchem-29 126 123 . . PUNCT eurjchem-29 126 124     SPACE eurjchem-29 127 1 also also ADV eurjchem-29 127 2 , , PUNCT eurjchem-29 127 3     SPACE eurjchem-29 127 4 the the DET eurjchem-29 127 5     SPACE eurjchem-29 127 6 presence presence NOUN eurjchem-29 127 7     SPACE eurjchem-29 127 8 of of ADP eurjchem-29 127 9     SPACE eurjchem-29 127 10 amino amino NOUN eurjchem-29 127 11     SPACE eurjchem-29 127 12 group group NOUN eurjchem-29 127 13     SPACE eurjchem-29 127 14 in in ADP eurjchem-29 127 15     SPACE eurjchem-29 127 16 compound compound NOUN eurjchem-29 127 17     SPACE eurjchem-29 127 18 8 8 NUM eurjchem-29 127 19     SPACE eurjchem-29 127 20 has have AUX eurjchem-29 127 21     SPACE eurjchem-29 127 22 been be AUX eurjchem-29 127 23     SPACE eurjchem-29 127 24 confirmed confirm VERB eurjchem-29 127 25         SPACE eurjchem-29 127 26 by by ADP eurjchem-29 127 27     SPACE eurjchem-29 127 28 acylation acylation NOUN eurjchem-29 127 29     SPACE eurjchem-29 127 30 with with ADP eurjchem-29 127 31     SPACE eurjchem-29 127 32 acetic acetic ADJ eurjchem-29 127 33     SPACE eurjchem-29 127 34 acid acid NOUN eurjchem-29 127 35     SPACE eurjchem-29 127 36 in in ADP eurjchem-29 127 37     SPACE eurjchem-29 127 38 the the DET eurjchem-29 127 39     SPACE eurjchem-29 127 40 presence presence NOUN eurjchem-29 127 41     SPACE eurjchem-29 127 42 of of ADP eurjchem-29 127 43     SPACE eurjchem-29 127 44 fused fuse VERB eurjchem-29 127 45     SPACE eurjchem-29 127 46 sodium sodium NOUN eurjchem-29 127 47     SPACE eurjchem-29 127 48 acetate acetate NOUN eurjchem-29 127 49     SPACE eurjchem-29 127 50 to to PART eurjchem-29 127 51     SPACE eurjchem-29 127 52 give give VERB eurjchem-29 127 53     SPACE eurjchem-29 127 54 the the DET eurjchem-29 127 55     SPACE eurjchem-29 127 56 acetamide acetamide NOUN eurjchem-29 127 57     SPACE eurjchem-29 127 58 derivative derivative NOUN eurjchem-29 127 59     SPACE eurjchem-29 127 60 9 9 NUM eurjchem-29 127 61     SPACE eurjchem-29 127 62 ( ( PUNCT eurjchem-29 127 63 scheme scheme NOUN eurjchem-29 127 64     SPACE eurjchem-29 127 65 2 2 NUM eurjchem-29 127 66 ) ) PUNCT eurjchem-29 127 67 . . PUNCT eurjchem-29 127 68     SPACE eurjchem-29 128 1 the the DET eurjchem-29 128 2     SPACE eurjchem-29 128 3 ir ir NOUN eurjchem-29 128 4     SPACE eurjchem-29 128 5 spectrum spectrum NOUN eurjchem-29 128 6     SPACE eurjchem-29 128 7 of of ADP eurjchem-29 128 8     SPACE eurjchem-29 128 9 9 9 NUM eurjchem-29 128 10     SPACE eurjchem-29 128 11 showed show VERB eurjchem-29 128 12     SPACE eurjchem-29 128 13 two two NUM eurjchem-29 128 14     SPACE eurjchem-29 128 15 characteristic characteristic ADJ eurjchem-29 128 16     SPACE eurjchem-29 128 17 absorption absorption NOUN eurjchem-29 128 18     SPACE eurjchem-29 128 19 bands band NOUN eurjchem-29 128 20     SPACE eurjchem-29 128 21 at at ADP eurjchem-29 128 22     SPACE eurjchem-29 128 23 3278 3278 NUM eurjchem-29 128 24     SPACE eurjchem-29 128 25 and and CCONJ eurjchem-29 128 26     SPACE eurjchem-29 128 27 2982 2982 NUM eurjchem-29 128 28     SPACE eurjchem-29 128 29 cm‐1 cm‐1 NOUN eurjchem-29 128 30     SPACE eurjchem-29 128 31 due due ADJ eurjchem-29 128 32     SPACE eurjchem-29 128 33 to to ADP eurjchem-29 128 34     SPACE eurjchem-29 128 35 nh nh NOUN eurjchem-29 128 36     SPACE eurjchem-29 128 37 and and CCONJ eurjchem-29 128 38     SPACE eurjchem-29 128 39 methyl methyl NOUN eurjchem-29 128 40     SPACE eurjchem-29 128 41 group group NOUN eurjchem-29 128 42     SPACE eurjchem-29 128 43 in in ADP eurjchem-29 128 44     SPACE eurjchem-29 128 45 addition addition NOUN eurjchem-29 128 46     SPACE eurjchem-29 128 47 to to ADP eurjchem-29 128 48     SPACE eurjchem-29 128 49 the the DET eurjchem-29 128 50     SPACE eurjchem-29 128 51 carbonyl carbonyl NOUN eurjchem-29 128 52     SPACE eurjchem-29 128 53 absorption absorption NOUN eurjchem-29 128 54     SPACE eurjchem-29 128 55 band band NOUN eurjchem-29 128 56     SPACE eurjchem-29 128 57 at at ADP eurjchem-29 128 58     SPACE eurjchem-29 128 59 1662 1662 NUM eurjchem-29 128 60     SPACE eurjchem-29 128 61 cm‐1 cm‐1 NOUN eurjchem-29 128 62 . . PUNCT eurjchem-29 128 63     SPACE eurjchem-29 129 1 its its PRON eurjchem-29 129 2     SPACE eurjchem-29 129 3 1h 1h NUM eurjchem-29 129 4     SPACE eurjchem-29 129 5 nmr nmr NOUN eurjchem-29 129 6     SPACE eurjchem-29 129 7 spectrum spectrum NOUN eurjchem-29 129 8     SPACE eurjchem-29 129 9 revealed reveal VERB eurjchem-29 129 10     SPACE eurjchem-29 129 11 two two NUM eurjchem-29 129 12     SPACE eurjchem-29 129 13 characteristic characteristic ADJ eurjchem-29 129 14     SPACE eurjchem-29 129 15 signals signal NOUN eurjchem-29 129 16     SPACE eurjchem-29 129 17 at at ADP eurjchem-29 129 18     SPACE eurjchem-29 129 19 8.78 8.78 NUM eurjchem-29 129 20     SPACE eurjchem-29 129 21 and and CCONJ eurjchem-29 129 22     SPACE eurjchem-29 129 23 9.37 9.37 NUM eurjchem-29 129 24     SPACE eurjchem-29 129 25 ppm ppm AUX eurjchem-29 129 26     SPACE eurjchem-29 129 27 assigned assign VERB eurjchem-29 129 28     SPACE eurjchem-29 129 29 to to ADP eurjchem-29 129 30     SPACE eurjchem-29 129 31 two two NUM eurjchem-29 129 32     SPACE eurjchem-29 129 33 nh nh NOUN eurjchem-29 129 34     SPACE eurjchem-29 129 35 protons proton NOUN eurjchem-29 129 36 . . PUNCT eurjchem-29 129 37     SPACE eurjchem-29 129 38 also also ADV eurjchem-29 129 39 , , PUNCT eurjchem-29 129 40     SPACE eurjchem-29 129 41 its its PRON eurjchem-29 129 42     SPACE eurjchem-29 129 43 mass mass NOUN eurjchem-29 129 44     SPACE eurjchem-29 129 45 spectrum spectrum NOUN eurjchem-29 129 46     SPACE eurjchem-29 129 47 showed show VERB eurjchem-29 129 48     SPACE eurjchem-29 129 49 the the DET eurjchem-29 129 50     SPACE eurjchem-29 129 51 molecular molecular ADJ eurjchem-29 129 52     SPACE eurjchem-29 129 53 ion ion NOUN eurjchem-29 129 54     SPACE eurjchem-29 129 55 peak peak NOUN eurjchem-29 129 56     SPACE eurjchem-29 129 57 at at ADP eurjchem-29 129 58     SPACE eurjchem-29 129 59 m m PROPN eurjchem-29 129 60 / / PROPN eurjchem-29 130 1 z z NOUN eurjchem-29 130 2     SPACE eurjchem-29 130 3 719 719 NUM eurjchem-29 130 4     SPACE eurjchem-29 131 1 [ [ X eurjchem-29 131 2 m+ m+ NOUN eurjchem-29 131 3 ] ] X eurjchem-29 131 4     SPACE eurjchem-29 131 5 and and CCONJ eurjchem-29 131 6     SPACE eurjchem-29 131 7 the the DET eurjchem-29 131 8     SPACE eurjchem-29 131 9 base base NOUN eurjchem-29 131 10     SPACE eurjchem-29 131 11 peak peak NOUN eurjchem-29 131 12     SPACE eurjchem-29 131 13 at at ADP eurjchem-29 131 14     SPACE eurjchem-29 131 15 m m PROPN eurjchem-29 131 16 / / PROPN eurjchem-29 131 17 z z NOUN eurjchem-29 131 18     SPACE eurjchem-29 131 19 77 77 NUM eurjchem-29 131 20 . . PUNCT eurjchem-29 131 21       SPACE eurjchem-29 131 22 on on ADP eurjchem-29 131 23     SPACE eurjchem-29 131 24 the the DET eurjchem-29 131 25     SPACE eurjchem-29 131 26 other other ADJ eurjchem-29 131 27     SPACE eurjchem-29 131 28 hand hand NOUN eurjchem-29 131 29 , , PUNCT eurjchem-29 131 30     SPACE eurjchem-29 131 31 alkylation alkylation NOUN eurjchem-29 131 32     SPACE eurjchem-29 131 33 of of ADP eurjchem-29 131 34     SPACE eurjchem-29 131 35 compound compound NOUN eurjchem-29 131 36     SPACE eurjchem-29 131 37 6a 6a NOUN eurjchem-29 131 38     SPACE eurjchem-29 131 39 with with ADP eurjchem-29 131 40     SPACE eurjchem-29 131 41 ethyl ethyl NOUN eurjchem-29 131 42     SPACE eurjchem-29 131 43 chloroacetate chloroacetate NOUN eurjchem-29 131 44     SPACE eurjchem-29 131 45 in in ADP eurjchem-29 131 46     SPACE eurjchem-29 131 47 the the DET eurjchem-29 131 48     SPACE eurjchem-29 131 49 presence presence NOUN eurjchem-29 131 50     SPACE eurjchem-29 131 51 of of ADP eurjchem-29 131 52     SPACE eurjchem-29 131 53 dmf dmf PROPN eurjchem-29 131 54     SPACE eurjchem-29 131 55 produced produce VERB eurjchem-29 131 56     SPACE eurjchem-29 131 57 10 10 NUM eurjchem-29 131 58 , , PUNCT eurjchem-29 131 59     SPACE eurjchem-29 131 60 which which PRON eurjchem-29 131 61     SPACE eurjchem-29 131 62 on on ADP eurjchem-29 131 63     SPACE eurjchem-29 131 64 refluxing refluxing NOUN eurjchem-29 131 65     SPACE eurjchem-29 131 66 with with ADP eurjchem-29 131 67     SPACE eurjchem-29 131 68 hydrazine hydrazine NOUN eurjchem-29 131 69     SPACE eurjchem-29 131 70 hydrate hydrate NOUN eurjchem-29 131 71     SPACE eurjchem-29 131 72 in in ADP eurjchem-29 131 73     SPACE eurjchem-29 131 74 absolute absolute ADJ eurjchem-29 131 75     SPACE eurjchem-29 131 76 ethanol ethanol NOUN eurjchem-29 131 77     SPACE eurjchem-29 131 78 yielded yield VERB eurjchem-29 131 79     SPACE eurjchem-29 131 80 the the DET eurjchem-29 131 81     SPACE eurjchem-29 131 82 carbohydrazide carbohydrazide NOUN eurjchem-29 131 83     SPACE eurjchem-29 131 84 derivative derivative NOUN eurjchem-29 131 85     SPACE eurjchem-29 131 86 11 11 NUM eurjchem-29 131 87 . . PUNCT eurjchem-29 131 88     SPACE eurjchem-29 131 89 treatment treatment NOUN eurjchem-29 131 90     SPACE eurjchem-29 131 91 of of ADP eurjchem-29 131 92     SPACE eurjchem-29 131 93 the the DET eurjchem-29 131 94     SPACE eurjchem-29 131 95 latter latter ADJ eurjchem-29 131 96     SPACE eurjchem-29 131 97 compound compound NOUN eurjchem-29 131 98     SPACE eurjchem-29 131 99 with with ADP eurjchem-29 131 100     SPACE eurjchem-29 131 101 ammonium ammonium NOUN eurjchem-29 131 102     SPACE eurjchem-29 131 103 thiocyanate thiocyanate NOUN eurjchem-29 131 104     SPACE eurjchem-29 131 105 afforded afford VERB eurjchem-29 131 106     SPACE eurjchem-29 131 107 acylthio acylthio NOUN eurjchem-29 131 108     SPACE eurjchem-29 131 109 semicarbazide semicarbazide NOUN eurjchem-29 131 110     SPACE eurjchem-29 131 111 derivative derivative NOUN eurjchem-29 131 112     SPACE eurjchem-29 131 113 12 12 NUM eurjchem-29 131 114 . . PUNCT eurjchem-29 131 115     SPACE eurjchem-29 131 116 an an DET eurjchem-29 131 117     SPACE eurjchem-29 131 118 intramolecular intramolecular ADJ eurjchem-29 131 119     SPACE eurjchem-29 131 120 cycloconden‐ cycloconden‐ NOUN eurjchem-29 131 121 sation sation NOUN eurjchem-29 131 122     SPACE eurjchem-29 131 123 of of ADP eurjchem-29 131 124     SPACE eurjchem-29 131 125 12 12 NUM eurjchem-29 131 126     SPACE eurjchem-29 131 127 was be AUX eurjchem-29 131 128     SPACE eurjchem-29 131 129 carried carry VERB eurjchem-29 131 130     SPACE eurjchem-29 131 131 out out ADP eurjchem-29 131 132     SPACE eurjchem-29 131 133 by by ADP eurjchem-29 131 134     SPACE eurjchem-29 131 135 refluxing refluxing NOUN eurjchem-29 131 136     SPACE eurjchem-29 131 137 it it PRON eurjchem-29 131 138     SPACE eurjchem-29 131 139 in in ADP eurjchem-29 131 140     SPACE eurjchem-29 131 141 glacial glacial ADJ eurjchem-29 131 142     SPACE eurjchem-29 131 143 acetic acetic ADJ eurjchem-29 131 144     SPACE eurjchem-29 131 145 acid acid NOUN eurjchem-29 131 146     SPACE eurjchem-29 131 147 in in ADP eurjchem-29 131 148     SPACE eurjchem-29 131 149 the the DET eurjchem-29 131 150     SPACE eurjchem-29 131 151 presence presence NOUN eurjchem-29 131 152     SPACE eurjchem-29 131 153 of of ADP eurjchem-29 131 154     SPACE eurjchem-29 131 155 fused fuse VERB eurjchem-29 131 156     SPACE eurjchem-29 131 157 sodium sodium NOUN eurjchem-29 131 158     SPACE eurjchem-29 131 159 acetate acetate NOUN eurjchem-29 131 160     SPACE eurjchem-29 131 161 to to PART eurjchem-29 131 162     SPACE eurjchem-29 131 163 yield yield VERB eurjchem-29 131 164     SPACE eurjchem-29 131 165 5‐thioxo‐1,2,4‐ 5‐thioxo‐1,2,4‐ NUM eurjchem-29 131 166 trazolo trazolo NOUN eurjchem-29 131 167     SPACE eurjchem-29 131 168 pyridine pyridine NOUN eurjchem-29 131 169     SPACE eurjchem-29 131 170 derivative derivative NOUN eurjchem-29 131 171     SPACE eurjchem-29 131 172 13 13 NUM eurjchem-29 131 173     SPACE eurjchem-29 131 174 ( ( PUNCT eurjchem-29 131 175 scheme scheme NOUN eurjchem-29 131 176     SPACE eurjchem-29 131 177 2 2 NUM eurjchem-29 131 178 ) ) PUNCT eurjchem-29 131 179 . . PUNCT eurjchem-29 131 180     SPACE eurjchem-29 132 1 the the DET eurjchem-29 132 2     SPACE eurjchem-29 132 3 structures structure NOUN eurjchem-29 132 4     SPACE eurjchem-29 132 5 of of ADP eurjchem-29 132 6     SPACE eurjchem-29 132 7 compounds compound VERB eurjchem-29 132 8     SPACE eurjchem-29 132 9 10­13 10­13 NOUN eurjchem-29 132 10     SPACE eurjchem-29 132 11 were be AUX eurjchem-29 132 12     SPACE eurjchem-29 132 13 confirmed confirm VERB eurjchem-29 132 14     SPACE eurjchem-29 132 15 from from ADP eurjchem-29 132 16     SPACE eurjchem-29 132 17 elemental elemental ADJ eurjchem-29 132 18     SPACE eurjchem-29 132 19 analysis analysis NOUN eurjchem-29 132 20     SPACE eurjchem-29 132 21 and and CCONJ eurjchem-29 132 22     SPACE eurjchem-29 132 23 spectral spectral ADJ eurjchem-29 132 24     SPACE eurjchem-29 132 25 data datum NOUN eurjchem-29 132 26 . . PUNCT eurjchem-29 132 27     SPACE eurjchem-29 133 1 the the DET eurjchem-29 133 2     SPACE eurjchem-29 133 3 ir ir NOUN eurjchem-29 133 4     SPACE eurjchem-29 133 5 spectrum spectrum NOUN eurjchem-29 133 6     SPACE eurjchem-29 133 7 data datum NOUN eurjchem-29 133 8     SPACE eurjchem-29 133 9 of of ADP eurjchem-29 133 10     SPACE eurjchem-29 133 11 10 10 NUM eurjchem-29 133 12     SPACE eurjchem-29 133 13 showed show VERB eurjchem-29 133 14     SPACE eurjchem-29 133 15 disappearance disappearance NOUN eurjchem-29 133 16     SPACE eurjchem-29 133 17 of of ADP eurjchem-29 133 18     SPACE eurjchem-29 133 19 the the DET eurjchem-29 133 20     SPACE eurjchem-29 133 21 absorption absorption NOUN eurjchem-29 133 22     SPACE eurjchem-29 133 23 band band NOUN eurjchem-29 133 24     SPACE eurjchem-29 133 25 due due ADJ eurjchem-29 133 26     SPACE eurjchem-29 133 27 to to ADP eurjchem-29 133 28     SPACE eurjchem-29 133 29 nh nh PROPN eurjchem-29 133 30     SPACE eurjchem-29 133 31 group group NOUN eurjchem-29 133 32     SPACE eurjchem-29 133 33 with with ADP eurjchem-29 133 34     SPACE eurjchem-29 133 35 the the DET eurjchem-29 133 36     SPACE eurjchem-29 133 37 presence presence NOUN eurjchem-29 133 38     SPACE eurjchem-29 133 39 of of ADP eurjchem-29 133 40     SPACE eurjchem-29 133 41 new new ADJ eurjchem-29 133 42     SPACE eurjchem-29 133 43 absorption absorption NOUN eurjchem-29 133 44     SPACE eurjchem-29 133 45 band band NOUN eurjchem-29 133 46     SPACE eurjchem-29 133 47 at at ADP eurjchem-29 133 48     SPACE eurjchem-29 133 49 1685 1685 NUM eurjchem-29 133 50     SPACE eurjchem-29 133 51 cm‐1 cm‐1 NOUN eurjchem-29 133 52     SPACE eurjchem-29 133 53 for for ADP eurjchem-29 133 54     SPACE eurjchem-29 133 55 c c PROPN eurjchem-29 133 56 = = NOUN eurjchem-29 133 57 o o NOUN eurjchem-29 133 58     SPACE eurjchem-29 133 59 ester ester NOUN eurjchem-29 133 60     SPACE eurjchem-29 133 61 group group NOUN eurjchem-29 133 62 , , PUNCT eurjchem-29 133 63     SPACE eurjchem-29 133 64 while while SCONJ eurjchem-29 133 65     SPACE eurjchem-29 133 66 that that PRON eurjchem-29 133 67     SPACE eurjchem-29 133 68 of of ADP eurjchem-29 133 69     SPACE eurjchem-29 133 70 11 11 NUM eurjchem-29 133 71     SPACE eurjchem-29 133 72 showed show VERB eurjchem-29 133 73     SPACE eurjchem-29 133 74 absorption absorption NOUN eurjchem-29 133 75     SPACE eurjchem-29 133 76 bands band NOUN eurjchem-29 133 77     SPACE eurjchem-29 133 78 at at ADP eurjchem-29 133 79     SPACE eurjchem-29 133 80 3327 3327 NUM eurjchem-29 133 81 , , PUNCT eurjchem-29 133 82     SPACE eurjchem-29 133 83 3229 3229 NUM eurjchem-29 133 84     SPACE eurjchem-29 133 85 and and CCONJ eurjchem-29 133 86     SPACE eurjchem-29 133 87 1663 1663 NUM eurjchem-29 133 88       SPACE eurjchem-29 133 89 cm‐1 cm‐1 NOUN eurjchem-29 133 90     SPACE eurjchem-29 133 91 due due ADJ eurjchem-29 133 92     SPACE eurjchem-29 133 93 to to PART eurjchem-29 133 94     SPACE eurjchem-29 133 95 nh2 nh2 PROPN eurjchem-29 133 96 , , PUNCT eurjchem-29 133 97     SPACE eurjchem-29 133 98 nh nh NOUN eurjchem-29 133 99     SPACE eurjchem-29 133 100 and and CCONJ eurjchem-29 133 101     SPACE eurjchem-29 133 102 c c NOUN eurjchem-29 133 103 = = NOUN eurjchem-29 133 104 o o NOUN eurjchem-29 133 105     SPACE eurjchem-29 133 106 groups group NOUN eurjchem-29 133 107 , , PUNCT eurjchem-29 133 108     SPACE eurjchem-29 133 109 respectively respectively ADV eurjchem-29 133 110 . . PUNCT eurjchem-29 133 111     SPACE eurjchem-29 133 112 on on ADP eurjchem-29 133 113     SPACE eurjchem-29 133 114 the the DET eurjchem-29 133 115     SPACE eurjchem-29 133 116 other other ADJ eurjchem-29 133 117     SPACE eurjchem-29 133 118 hand hand NOUN eurjchem-29 133 119 , , PUNCT eurjchem-29 133 120     SPACE eurjchem-29 133 121 the the DET eurjchem-29 133 122     SPACE eurjchem-29 133 123 structure structure NOUN eurjchem-29 133 124     SPACE eurjchem-29 133 125 of of ADP eurjchem-29 133 126     SPACE eurjchem-29 133 127 13 13 NUM eurjchem-29 133 128     SPACE eurjchem-29 133 129 was be AUX eurjchem-29 133 130     SPACE eurjchem-29 133 131 elucidated elucidated ADJ eurjchem-29 133 132     SPACE eurjchem-29 133 133 on on ADP eurjchem-29 133 134     SPACE eurjchem-29 133 135 the the DET eurjchem-29 133 136     SPACE eurjchem-29 133 137 basis basis NOUN eurjchem-29 133 138     SPACE eurjchem-29 133 139 of of ADP eurjchem-29 133 140     SPACE eurjchem-29 133 141 elemental elemental ADJ eurjchem-29 133 142     SPACE eurjchem-29 133 143 analysis analysis NOUN eurjchem-29 133 144     SPACE eurjchem-29 133 145 and and CCONJ eurjchem-29 133 146     SPACE eurjchem-29 133 147 spectral spectral ADJ eurjchem-29 133 148     SPACE eurjchem-29 133 149 data datum NOUN eurjchem-29 133 150 . . PUNCT eurjchem-29 133 151     SPACE eurjchem-29 134 1 its its PRON eurjchem-29 134 2     SPACE eurjchem-29 134 3 ir ir NOUN eurjchem-29 134 4     SPACE eurjchem-29 134 5 spectrum spectrum NOUN eurjchem-29 134 6     SPACE eurjchem-29 134 7 showed show VERB eurjchem-29 134 8     SPACE eurjchem-29 134 9 absorption absorption NOUN eurjchem-29 134 10     SPACE eurjchem-29 134 11 bands band NOUN eurjchem-29 134 12     SPACE eurjchem-29 134 13 at at ADP eurjchem-29 134 14     SPACE eurjchem-29 134 15 3212 3212 NUM eurjchem-29 134 16 , , PUNCT eurjchem-29 134 17     SPACE eurjchem-29 134 18 3209 3209 NUM eurjchem-29 134 19     SPACE eurjchem-29 134 20 and and CCONJ eurjchem-29 134 21     SPACE eurjchem-29 134 22 3184 3184 NUM eurjchem-29 134 23     SPACE eurjchem-29 134 24 cm‐1 cm‐1 NOUN eurjchem-29 134 25     SPACE eurjchem-29 134 26 due due ADJ eurjchem-29 134 27     SPACE eurjchem-29 134 28 to to ADP eurjchem-29 134 29     SPACE eurjchem-29 134 30 three three NUM eurjchem-29 134 31     SPACE eurjchem-29 134 32 ( ( PUNCT eurjchem-29 134 33 nh nh NOUN eurjchem-29 134 34 ) ) PUNCT eurjchem-29 134 35     SPACE eurjchem-29 134 36 groups group NOUN eurjchem-29 134 37 , , PUNCT eurjchem-29 134 38     SPACE eurjchem-29 134 39 with with ADP eurjchem-29 134 40     SPACE eurjchem-29 134 41 absence absence NOUN eurjchem-29 134 42     SPACE eurjchem-29 134 43 of of ADP eurjchem-29 134 44     SPACE eurjchem-29 134 45 both both DET eurjchem-29 134 46     SPACE eurjchem-29 134 47 nh2 nh2 PROPN eurjchem-29 134 48     SPACE eurjchem-29 134 49 and and CCONJ eurjchem-29 134 50     SPACE eurjchem-29 134 51 c c NOUN eurjchem-29 134 52 = = NOUN eurjchem-29 134 53 o o NOUN eurjchem-29 134 54     SPACE eurjchem-29 134 55 bands band NOUN eurjchem-29 134 56     SPACE eurjchem-29 134 57 which which PRON eurjchem-29 134 58     SPACE eurjchem-29 134 59 revealed reveal VERB eurjchem-29 134 60     SPACE eurjchem-29 134 61 that that SCONJ eurjchem-29 134 62     SPACE eurjchem-29 134 63 cyclocondensation cyclocondensation NOUN eurjchem-29 134 64     SPACE eurjchem-29 134 65 has have AUX eurjchem-29 134 66     SPACE eurjchem-29 134 67 occurred occur VERB eurjchem-29 134 68     SPACE eurjchem-29 134 69 between between ADP eurjchem-29 134 70     SPACE eurjchem-29 134 71 nh2 nh2 NOUN eurjchem-29 134 72     SPACE eurjchem-29 134 73 and and CCONJ eurjchem-29 134 74     SPACE eurjchem-29 134 75 c c NOUN eurjchem-29 134 76 = = NOUN eurjchem-29 134 77 o o NOUN eurjchem-29 134 78     SPACE eurjchem-29 134 79 in in ADP eurjchem-29 134 80     SPACE eurjchem-29 134 81 the the DET eurjchem-29 134 82     SPACE eurjchem-29 134 83 side side NOUN eurjchem-29 134 84     SPACE eurjchem-29 134 85 chain chain NOUN eurjchem-29 134 86     SPACE eurjchem-29 134 87 of of ADP eurjchem-29 134 88     SPACE eurjchem-29 134 89 acylthio‐ acylthio‐ NOUN eurjchem-29 134 90 semicarbazide semicarbazide NOUN eurjchem-29 134 91     SPACE eurjchem-29 134 92 12 12 NUM eurjchem-29 134 93 . . PUNCT eurjchem-29 134 94     SPACE eurjchem-29 134 95 its its PRON eurjchem-29 134 96     SPACE eurjchem-29 134 97 1h 1h NUM eurjchem-29 134 98     SPACE eurjchem-29 134 99 nmr nmr NOUN eurjchem-29 134 100     SPACE eurjchem-29 134 101 spectrum spectrum NOUN eurjchem-29 134 102     SPACE eurjchem-29 134 103 revealed reveal VERB eurjchem-29 134 104     SPACE eurjchem-29 134 105 the the DET eurjchem-29 134 106     SPACE eurjchem-29 134 107 appearance appearance NOUN eurjchem-29 134 108     SPACE eurjchem-29 134 109 of of ADP eurjchem-29 134 110     SPACE eurjchem-29 134 111 singlets singlet NOUN eurjchem-29 134 112     SPACE eurjchem-29 134 113 at at ADP eurjchem-29 134 114     SPACE eurjchem-29 134 115 8.96 8.96 NUM eurjchem-29 134 116 , , PUNCT eurjchem-29 134 117     SPACE eurjchem-29 134 118 9.57 9.57 NUM eurjchem-29 134 119 , , PUNCT eurjchem-29 134 120     SPACE eurjchem-29 134 121 9.89 9.89 NUM eurjchem-29 134 122     SPACE eurjchem-29 134 123 ppm ppm NOUN eurjchem-29 134 124     SPACE eurjchem-29 134 125 due due ADJ eurjchem-29 134 126     SPACE eurjchem-29 134 127 to to ADP eurjchem-29 134 128     SPACE eurjchem-29 134 129 three three NUM eurjchem-29 134 130     SPACE eurjchem-29 134 131 different different ADJ eurjchem-29 134 132     SPACE eurjchem-29 134 133 nh nh NOUN eurjchem-29 134 134     SPACE eurjchem-29 134 135 protons proton NOUN eurjchem-29 134 136 . . PUNCT eurjchem-29 134 137         SPACE eurjchem-29 134 138 3.2 3.2 NUM eurjchem-29 134 139 . . PUNCT eurjchem-29 134 140     SPACE eurjchem-29 134 141 antimicrobial antimicrobial ADJ eurjchem-29 134 142     SPACE eurjchem-29 134 143 activities activity NOUN eurjchem-29 134 144         SPACE eurjchem-29 134 145 the the DET eurjchem-29 134 146     SPACE eurjchem-29 134 147 results result NOUN eurjchem-29 134 148     SPACE eurjchem-29 134 149 of of ADP eurjchem-29 134 150     SPACE eurjchem-29 134 151 the the DET eurjchem-29 134 152     SPACE eurjchem-29 134 153 biological biological ADJ eurjchem-29 134 154     SPACE eurjchem-29 134 155 studies study NOUN eurjchem-29 134 156     SPACE eurjchem-29 134 157 are be AUX eurjchem-29 134 158     SPACE eurjchem-29 134 159 summarized summarize VERB eurjchem-29 134 160     SPACE eurjchem-29 134 161 in in ADP eurjchem-29 134 162     SPACE eurjchem-29 134 163 table table NOUN eurjchem-29 134 164     SPACE eurjchem-29 134 165 1 1 NUM eurjchem-29 134 166 . . PUNCT eurjchem-29 134 167     SPACE eurjchem-29 134 168 from from ADP eurjchem-29 134 169     SPACE eurjchem-29 134 170 the the DET eurjchem-29 134 171     SPACE eurjchem-29 134 172 data datum NOUN eurjchem-29 134 173     SPACE eurjchem-29 134 174 it it PRON eurjchem-29 134 175     SPACE eurjchem-29 134 176 is be AUX eurjchem-29 134 177     SPACE eurjchem-29 134 178 clear clear ADJ eurjchem-29 134 179     SPACE eurjchem-29 134 180 that that SCONJ eurjchem-29 134 181     SPACE eurjchem-29 134 182 most most ADJ eurjchem-29 134 183     SPACE eurjchem-29 134 184 of of ADP eurjchem-29 134 185     SPACE eurjchem-29 134 186 the the DET eurjchem-29 134 187     SPACE eurjchem-29 134 188 synthesized synthesize VERB eurjchem-29 134 189     SPACE eurjchem-29 134 190 compounds compound NOUN eurjchem-29 134 191     SPACE eurjchem-29 134 192 were be AUX eurjchem-29 134 193     SPACE eurjchem-29 134 194 found find VERB eurjchem-29 134 195     SPACE eurjchem-29 134 196 to to PART eurjchem-29 134 197     SPACE eurjchem-29 134 198 possess possess VERB eurjchem-29 134 199     SPACE eurjchem-29 134 200 various various ADJ eurjchem-29 134 201     SPACE eurjchem-29 134 202 antimicrobial antimicrobial ADJ eurjchem-29 134 203     SPACE eurjchem-29 134 204 activities activity NOUN eurjchem-29 134 205     SPACE eurjchem-29 134 206 towards towards ADP eurjchem-29 134 207     SPACE eurjchem-29 134 208 all all DET eurjchem-29 134 209     SPACE eurjchem-29 134 210 the the DET eurjchem-29 134 211     SPACE eurjchem-29 134 212 microorganisms microorganism NOUN eurjchem-29 134 213     SPACE eurjchem-29 134 214 tested test VERB eurjchem-29 134 215 . . PUNCT eurjchem-29 134 216     SPACE eurjchem-29 134 217 the the DET eurjchem-29 134 218     SPACE eurjchem-29 134 219 antimicrobial antimicrobial ADJ eurjchem-29 134 220     SPACE eurjchem-29 134 221 activities activity NOUN eurjchem-29 134 222     SPACE eurjchem-29 134 223 are be AUX eurjchem-29 134 224     SPACE eurjchem-29 134 225 carried carry VERB eurjchem-29 134 226     SPACE eurjchem-29 134 227 out out ADP eurjchem-29 134 228     SPACE eurjchem-29 134 229 against against ADP eurjchem-29 134 230     SPACE eurjchem-29 134 231 two two NUM eurjchem-29 134 232     SPACE eurjchem-29 134 233 bacterial bacterial ADJ eurjchem-29 134 234     SPACE eurjchem-29 134 235 strains strain NOUN eurjchem-29 134 236 , , PUNCT eurjchem-29 134 237     SPACE eurjchem-29 134 238 b. b. NOUN eurjchem-29 134 239     SPACE eurjchem-29 134 240 subtilis subtilis PROPN eurjchem-29 134 241     SPACE eurjchem-29 134 242 and and CCONJ eurjchem-29 134 243     SPACE eurjchem-29 134 244 e. e. PROPN eurjchem-29 134 245     SPACE eurjchem-29 134 246 coli coli NOUN eurjchem-29 134 247     SPACE eurjchem-29 134 248 and and CCONJ eurjchem-29 134 249     SPACE eurjchem-29 134 250 two two NUM eurjchem-29 134 251     SPACE eurjchem-29 134 252 fungal fungal ADJ eurjchem-29 134 253     SPACE eurjchem-29 134 254 strains strain NOUN eurjchem-29 134 255 , , PUNCT eurjchem-29 134 256     SPACE eurjchem-29 134 257 namely namely ADV eurjchem-29 134 258     SPACE eurjchem-29 134 259 a. a. NOUN eurjchem-29 134 260     SPACE eurjchem-29 134 261 172 172 NUM eurjchem-29 134 262     SPACE eurjchem-29 134 263 abdel­monem abdel­monem NOUN eurjchem-29 134 264     SPACE eurjchem-29 134 265 / / SYM eurjchem-29 134 266     SPACE eurjchem-29 134 267 european european ADJ eurjchem-29 134 268     SPACE eurjchem-29 134 269 journal journal NOUN eurjchem-29 134 270     SPACE eurjchem-29 134 271 of of ADP eurjchem-29 134 272     SPACE eurjchem-29 134 273 chemistry chemistry NOUN eurjchem-29 134 274     SPACE eurjchem-29 134 275 1 1 NUM eurjchem-29 134 276     SPACE eurjchem-29 134 277 ( ( PUNCT eurjchem-29 134 278 3 3 NUM eurjchem-29 134 279 ) ) PUNCT eurjchem-29 134 280     SPACE eurjchem-29 134 281 ( ( PUNCT eurjchem-29 134 282 2010 2010 NUM eurjchem-29 134 283 ) ) PUNCT eurjchem-29 134 284     SPACE eurjchem-29 134 285 168­172 168­172 PRON eurjchem-29 134 286         SPACE eurjchem-29 134 287 fumigates fumigate NOUN eurjchem-29 134 288     SPACE eurjchem-29 134 289 and and CCONJ eurjchem-29 134 290     SPACE eurjchem-29 134 291 c. c. NOUN eurjchem-29 134 292     SPACE eurjchem-29 134 293 albicans albican NOUN eurjchem-29 134 294 . . PUNCT eurjchem-29 134 295     SPACE eurjchem-29 134 296 in in ADP eurjchem-29 134 297     SPACE eurjchem-29 134 298 general general ADJ eurjchem-29 134 299 , , PUNCT eurjchem-29 134 300     SPACE eurjchem-29 134 301 most most ADJ eurjchem-29 134 302     SPACE eurjchem-29 134 303 of of ADP eurjchem-29 134 304     SPACE eurjchem-29 134 305 the the DET eurjchem-29 134 306     SPACE eurjchem-29 134 307 synthesized synthesize VERB eurjchem-29 134 308     SPACE eurjchem-29 134 309 compounds compound NOUN eurjchem-29 134 310     SPACE eurjchem-29 134 311 showed show VERB eurjchem-29 134 312     SPACE eurjchem-29 134 313 a a DET eurjchem-29 134 314     SPACE eurjchem-29 134 315 greater great ADJ eurjchem-29 134 316     SPACE eurjchem-29 134 317 inhibitory inhibitory ADJ eurjchem-29 134 318     SPACE eurjchem-29 134 319 effect effect NOUN eurjchem-29 134 320     SPACE eurjchem-29 134 321 against against ADP eurjchem-29 134 322     SPACE eurjchem-29 134 323 both both PRON eurjchem-29 134 324     SPACE eurjchem-29 134 325 the the DET eurjchem-29 134 326     SPACE eurjchem-29 134 327 bacterial bacterial ADJ eurjchem-29 134 328     SPACE eurjchem-29 134 329 and and CCONJ eurjchem-29 134 330     SPACE eurjchem-29 134 331 fungal fungal ADJ eurjchem-29 134 332     SPACE eurjchem-29 134 333 strains strain NOUN eurjchem-29 134 334     SPACE eurjchem-29 134 335 compared compare VERB eurjchem-29 134 336     SPACE eurjchem-29 134 337 to to ADP eurjchem-29 134 338     SPACE eurjchem-29 134 339 the the DET eurjchem-29 134 340     SPACE eurjchem-29 134 341 starting starting NOUN eurjchem-29 134 342     SPACE eurjchem-29 134 343 material material NOUN eurjchem-29 134 344     SPACE eurjchem-29 134 345 3 3 NUM eurjchem-29 134 346     SPACE eurjchem-29 134 347 which which PRON eurjchem-29 134 348     SPACE eurjchem-29 134 349 confirmed confirm VERB eurjchem-29 134 350     SPACE eurjchem-29 134 351 improving improve VERB eurjchem-29 134 352     SPACE eurjchem-29 134 353 biological biological ADJ eurjchem-29 134 354     SPACE eurjchem-29 134 355 properties property NOUN eurjchem-29 134 356 . . PUNCT eurjchem-29 134 357     SPACE eurjchem-29 135 1 however however ADV eurjchem-29 135 2 , , PUNCT eurjchem-29 135 3     SPACE eurjchem-29 135 4 compound compound NOUN eurjchem-29 135 5     SPACE eurjchem-29 135 6 10 10 NUM eurjchem-29 135 7     SPACE eurjchem-29 135 8 showed show VERB eurjchem-29 135 9     SPACE eurjchem-29 135 10 maximum maximum ADJ eurjchem-29 135 11     SPACE eurjchem-29 135 12 antimicrobial antimicrobial ADJ eurjchem-29 135 13     SPACE eurjchem-29 135 14 activity activity NOUN eurjchem-29 135 15     SPACE eurjchem-29 135 16 comparable comparable ADJ eurjchem-29 135 17     SPACE eurjchem-29 135 18 to to ADP eurjchem-29 135 19     SPACE eurjchem-29 135 20 the the DET eurjchem-29 135 21     SPACE eurjchem-29 135 22 standard standard ADJ eurjchem-29 135 23     SPACE eurjchem-29 135 24 drugs drug NOUN eurjchem-29 135 25 . . PUNCT eurjchem-29 135 26     SPACE eurjchem-29 136 1 we we PRON eurjchem-29 136 2     SPACE eurjchem-29 136 3 can can AUX eurjchem-29 136 4     SPACE eurjchem-29 136 5 conclude conclude VERB eurjchem-29 136 6     SPACE eurjchem-29 136 7 form form NOUN eurjchem-29 136 8     SPACE eurjchem-29 136 9 the the DET eurjchem-29 136 10     SPACE eurjchem-29 136 11 preliminary preliminary ADJ eurjchem-29 136 12     SPACE eurjchem-29 136 13 antimicrobial antimicrobial ADJ eurjchem-29 136 14     SPACE eurjchem-29 136 15 screening screening NOUN eurjchem-29 136 16     SPACE eurjchem-29 136 17 that that SCONJ eurjchem-29 136 18     SPACE eurjchem-29 136 19 the the DET eurjchem-29 136 20     SPACE eurjchem-29 136 21 compounds compound NOUN eurjchem-29 136 22     SPACE eurjchem-29 136 23 5a 5a NUM eurjchem-29 136 24 , , PUNCT eurjchem-29 136 25     SPACE eurjchem-29 136 26 6a 6a NOUN eurjchem-29 136 27 , , PUNCT eurjchem-29 136 28     SPACE eurjchem-29 136 29 7 7 NUM eurjchem-29 136 30 , , PUNCT eurjchem-29 136 31     SPACE eurjchem-29 136 32 9 9 NUM eurjchem-29 136 33 , , PUNCT eurjchem-29 136 34     SPACE eurjchem-29 136 35 10 10 NUM eurjchem-29 136 36     SPACE eurjchem-29 136 37 and and CCONJ eurjchem-29 136 38     SPACE eurjchem-29 136 39 13 13 NUM eurjchem-29 136 40     SPACE eurjchem-29 136 41 enhance enhance VERB eurjchem-29 136 42     SPACE eurjchem-29 136 43 the the DET eurjchem-29 136 44     SPACE eurjchem-29 136 45 biological biological ADJ eurjchem-29 136 46     SPACE eurjchem-29 136 47 properties property NOUN eurjchem-29 136 48     SPACE eurjchem-29 136 49 due due ADJ eurjchem-29 136 50     SPACE eurjchem-29 136 51 to to ADP eurjchem-29 136 52     SPACE eurjchem-29 136 53 the the DET eurjchem-29 136 54     SPACE eurjchem-29 136 55 presence presence NOUN eurjchem-29 136 56     SPACE eurjchem-29 136 57 of of ADP eurjchem-29 136 58     SPACE eurjchem-29 136 59 bioactive bioactive NOUN eurjchem-29 136 60     SPACE eurjchem-29 136 61 moieties moiety NOUN eurjchem-29 136 62     SPACE eurjchem-29 136 63 as as ADP eurjchem-29 136 64     SPACE eurjchem-29 136 65 1,2,4‐triazol 1,2,4‐triazol NUM eurjchem-29 136 66     SPACE eurjchem-29 136 67 and and CCONJ eurjchem-29 136 68     SPACE eurjchem-29 136 69 1,2,4‐ 1,2,4‐ NUM eurjchem-29 136 70 triazine triazine NOUN eurjchem-29 136 71 . . PUNCT eurjchem-29 136 72         SPACE eurjchem-29 136 73 table table NOUN eurjchem-29 136 74     SPACE eurjchem-29 136 75 1 1 NUM eurjchem-29 136 76 . . PUNCT eurjchem-29 136 77     SPACE eurjchem-29 136 78 antibacterial antibacterial ADJ eurjchem-29 136 79     SPACE eurjchem-29 136 80 and and CCONJ eurjchem-29 136 81     SPACE eurjchem-29 136 82 antifungal antifungal ADJ eurjchem-29 136 83     SPACE eurjchem-29 136 84 activity activity NOUN eurjchem-29 136 85     SPACE eurjchem-29 136 86 data datum NOUN eurjchem-29 136 87 * * PROPN eurjchem-29 136 88 . . PUNCT eurjchem-29 136 89     SPACE eurjchem-29 136 90 compound compound VERB eurjchem-29 136 91     SPACE eurjchem-29 136 92 no no DET eurjchem-29 136 93     SPACE eurjchem-29 136 94 antibacterial antibacterial ADJ eurjchem-29 136 95     SPACE eurjchem-29 136 96 activity activity NOUN eurjchem-29 136 97       SPACE eurjchem-29 136 98 antifungal antifungal ADJ eurjchem-29 136 99     SPACE eurjchem-29 136 100 activity activity NOUN eurjchem-29 136 101     SPACE eurjchem-29 136 102 gram gram NOUN eurjchem-29 136 103     SPACE eurjchem-29 136 104 + + NOUN eurjchem-29 136 105     SPACE eurjchem-29 136 106 gram gram NOUN eurjchem-29 136 107     SPACE eurjchem-29 136 108 ­ ­ NOUN eurjchem-29 136 109     SPACE eurjchem-29 136 110 aspergillus aspergillus NOUN eurjchem-29 136 111     SPACE eurjchem-29 136 112 fumigatus fumigatus NOUN eurjchem-29 136 113     SPACE eurjchem-29 136 114 candida candida NOUN eurjchem-29 136 115     SPACE eurjchem-29 136 116 albicans albican NOUN eurjchem-29 136 117     SPACE eurjchem-29 136 118 bacillus bacillus NOUN eurjchem-29 136 119     SPACE eurjchem-29 136 120 subtilis subtili NOUN eurjchem-29 136 121     SPACE eurjchem-29 136 122 escherichia escherichia NOUN eurjchem-29 136 123     SPACE eurjchem-29 136 124 coli coli NOUN eurjchem-29 136 125     SPACE eurjchem-29 136 126 2a 2a NUM eurjchem-29 136 127     SPACE eurjchem-29 136 128 + + ADJ eurjchem-29 136 129 + + NOUN eurjchem-29 136 130     SPACE eurjchem-29 136 131 + + ADJ eurjchem-29 136 132 + + NOUN eurjchem-29 136 133     SPACE eurjchem-29 136 134 + + NOUN eurjchem-29 136 135     SPACE eurjchem-29 136 136 + + NOUN eurjchem-29 136 137     SPACE eurjchem-29 136 138 3a 3a NUM eurjchem-29 136 139     SPACE eurjchem-29 136 140 + + NOUN eurjchem-29 136 141     SPACE eurjchem-29 136 142 + + NOUN eurjchem-29 136 143     SPACE eurjchem-29 136 144 + + NOUN eurjchem-29 136 145     SPACE eurjchem-29 136 146 + + NOUN eurjchem-29 136 147     SPACE eurjchem-29 136 148 5a 5a NUM eurjchem-29 136 149     SPACE eurjchem-29 136 150 + + NOUN eurjchem-29 136 151     SPACE eurjchem-29 136 152 + + ADJ eurjchem-29 136 153 + + NOUN eurjchem-29 136 154     SPACE eurjchem-29 136 155 + + NOUN eurjchem-29 136 156     SPACE eurjchem-29 136 157 + + ADJ eurjchem-29 136 158 + + NOUN eurjchem-29 136 159     SPACE eurjchem-29 136 160 5b 5b NOUN eurjchem-29 136 161     SPACE eurjchem-29 136 162 + + NOUN eurjchem-29 136 163     SPACE eurjchem-29 136 164 + + NOUN eurjchem-29 136 165     SPACE eurjchem-29 136 166 + + NOUN eurjchem-29 136 167     SPACE eurjchem-29 136 168 + + NOUN eurjchem-29 136 169     SPACE eurjchem-29 136 170 6a 6a NOUN eurjchem-29 136 171     SPACE eurjchem-29 136 172 + + PROPN eurjchem-29 136 173 + + NOUN eurjchem-29 136 174     SPACE eurjchem-29 136 175 + + NOUN eurjchem-29 136 176     SPACE eurjchem-29 136 177 + + ADJ eurjchem-29 136 178 + + NOUN eurjchem-29 136 179     SPACE eurjchem-29 136 180 + + ADJ eurjchem-29 136 181 + + ADJ eurjchem-29 136 182     SPACE eurjchem-29 136 183 6b 6b NOUN eurjchem-29 136 184     SPACE eurjchem-29 136 185 + + PROPN eurjchem-29 136 186 + + NOUN eurjchem-29 136 187     SPACE eurjchem-29 136 188 + + ADJ eurjchem-29 136 189 + + NOUN eurjchem-29 136 190     SPACE eurjchem-29 136 191 + + ADJ eurjchem-29 136 192 + + NOUN eurjchem-29 136 193     SPACE eurjchem-29 136 194 + + ADJ eurjchem-29 136 195 + + NOUN eurjchem-29 136 196     SPACE eurjchem-29 136 197 7 7 NUM eurjchem-29 136 198     SPACE eurjchem-29 136 199 + + NOUN eurjchem-29 136 200     SPACE eurjchem-29 136 201 + + NOUN eurjchem-29 136 202     SPACE eurjchem-29 136 203 + + NOUN eurjchem-29 136 204     SPACE eurjchem-29 136 205 + + NOUN eurjchem-29 136 206     SPACE eurjchem-29 136 207 8 8 NUM eurjchem-29 136 208     SPACE eurjchem-29 136 209 + + PROPN eurjchem-29 136 210 + + NOUN eurjchem-29 136 211     SPACE eurjchem-29 136 212 + + NOUN eurjchem-29 136 213     SPACE eurjchem-29 136 214 + + ADJ eurjchem-29 136 215 + + NOUN eurjchem-29 136 216     SPACE eurjchem-29 136 217 + + NOUN eurjchem-29 136 218     SPACE eurjchem-29 136 219 9 9 NUM eurjchem-29 136 220     SPACE eurjchem-29 136 221 + + NOUN eurjchem-29 136 222     SPACE eurjchem-29 136 223 + + NOUN eurjchem-29 136 224     SPACE eurjchem-29 136 225 + + NOUN eurjchem-29 136 226     SPACE eurjchem-29 136 227 + + NOUN eurjchem-29 136 228     SPACE eurjchem-29 136 229 10 10 NUM eurjchem-29 136 230     SPACE eurjchem-29 136 231 + + PROPN eurjchem-29 136 232 + + ADJ eurjchem-29 136 233 + + NOUN eurjchem-29 136 234     SPACE eurjchem-29 136 235 + + ADJ eurjchem-29 136 236 + + NOUN eurjchem-29 136 237     SPACE eurjchem-29 136 238 + + ADJ eurjchem-29 136 239 + + NOUN eurjchem-29 136 240     SPACE eurjchem-29 136 241 + + NOUN eurjchem-29 136 242     SPACE eurjchem-29 136 243 11 11 NUM eurjchem-29 136 244     SPACE eurjchem-29 136 245 + + NOUN eurjchem-29 136 246     SPACE eurjchem-29 136 247 + + NOUN eurjchem-29 136 248     SPACE eurjchem-29 136 249 + + NOUN eurjchem-29 136 250     SPACE eurjchem-29 136 251 + + NOUN eurjchem-29 136 252     SPACE eurjchem-29 136 253 12 12 NUM eurjchem-29 136 254     SPACE eurjchem-29 136 255 + + PROPN eurjchem-29 136 256 + + NOUN eurjchem-29 136 257     SPACE eurjchem-29 136 258 + + NOUN eurjchem-29 136 259     SPACE eurjchem-29 136 260 + + NOUN eurjchem-29 136 261     SPACE eurjchem-29 136 262 + + NOUN eurjchem-29 136 263     SPACE eurjchem-29 136 264 13 13 NUM eurjchem-29 136 265     SPACE eurjchem-29 136 266 + + NOUN eurjchem-29 136 267     SPACE eurjchem-29 136 268 + + NOUN eurjchem-29 136 269     SPACE eurjchem-29 136 270 + + ADJ eurjchem-29 136 271 + + NOUN eurjchem-29 136 272     SPACE eurjchem-29 136 273 + + ADJ eurjchem-29 136 274 + + ADJ eurjchem-29 136 275     SPACE eurjchem-29 136 276 chloramphenicol chloramphenicol NOUN eurjchem-29 136 277     SPACE eurjchem-29 136 278 + + PROPN eurjchem-29 136 279 + + ADJ eurjchem-29 136 280 + + NOUN eurjchem-29 136 281     SPACE eurjchem-29 136 282 + + ADJ eurjchem-29 136 283 + + ADJ eurjchem-29 136 284 + + NOUN eurjchem-29 136 285     SPACE eurjchem-29 136 286 ‐ ‐ NOUN eurjchem-29 136 287     SPACE eurjchem-29 136 288 ‐ ‐ NOUN eurjchem-29 136 289     SPACE eurjchem-29 136 290 terbianfin terbianfin NOUN eurjchem-29 136 291       SPACE eurjchem-29 136 292 ‐ ‐ NOUN eurjchem-29 136 293     SPACE eurjchem-29 136 294 ‐ ‐ NOUN eurjchem-29 136 295     SPACE eurjchem-29 136 296 + + PROPN eurjchem-29 136 297 + + ADJ eurjchem-29 136 298 + + NOUN eurjchem-29 136 299     SPACE eurjchem-29 136 300 + + ADJ eurjchem-29 136 301 + + ADJ eurjchem-29 136 302     SPACE eurjchem-29 136 303 solvent solvent ADJ eurjchem-29 136 304     SPACE eurjchem-29 136 305 control control NOUN eurjchem-29 136 306     SPACE eurjchem-29 136 307 ( ( PUNCT eurjchem-29 136 308 dmf dmf PROPN eurjchem-29 136 309 ) ) PUNCT eurjchem-29 136 310     SPACE eurjchem-29 136 311 ‐ ‐ NOUN eurjchem-29 136 312     SPACE eurjchem-29 136 313 ‐ ‐ NOUN eurjchem-29 136 314     SPACE eurjchem-29 136 315 ‐ ‐ NOUN eurjchem-29 136 316     SPACE eurjchem-29 136 317 ‐ ‐ NOUN eurjchem-29 136 318     SPACE eurjchem-29 136 319 * * SYM eurjchem-29 136 320     SPACE eurjchem-29 136 321 the the DET eurjchem-29 136 322     SPACE eurjchem-29 136 323 test test NOUN eurjchem-29 136 324     SPACE eurjchem-29 136 325 done do VERB eurjchem-29 136 326     SPACE eurjchem-29 136 327 using use VERB eurjchem-29 136 328     SPACE eurjchem-29 136 329 the the DET eurjchem-29 136 330     SPACE eurjchem-29 136 331 diffusion diffusion NOUN eurjchem-29 136 332     SPACE eurjchem-29 136 333 agar agar NOUN eurjchem-29 136 334     SPACE eurjchem-29 136 335 technique technique NOUN eurjchem-29 136 336 : : PUNCT eurjchem-29 136 337     SPACE eurjchem-29 136 338 well well ADV eurjchem-29 136 339     SPACE eurjchem-29 136 340 diameter diameter NOUN eurjchem-29 136 341     SPACE eurjchem-29 136 342 = = NOUN eurjchem-29 136 343     SPACE eurjchem-29 136 344 0.06 0.06 NUM eurjchem-29 136 345     SPACE eurjchem-29 136 346 cm cm NOUN eurjchem-29 136 347 ; ; PUNCT eurjchem-29 136 348     SPACE eurjchem-29 136 349 inhibition inhibition NOUN eurjchem-29 136 350     SPACE eurjchem-29 136 351 values value NOUN eurjchem-29 136 352     SPACE eurjchem-29 136 353 = = NOUN eurjchem-29 136 354     SPACE eurjchem-29 136 355 0.1–0.5 0.1–0.5 NOUN eurjchem-29 136 356     SPACE eurjchem-29 136 357 cm cm NOUN eurjchem-29 136 358     SPACE eurjchem-29 136 359 beyond beyond ADP eurjchem-29 136 360     SPACE eurjchem-29 136 361 control control NOUN eurjchem-29 136 362     SPACE eurjchem-29 136 363 = = NOUN eurjchem-29 136 364     SPACE eurjchem-29 136 365 + + NOUN eurjchem-29 136 366     SPACE eurjchem-29 136 367 ( ( PUNCT eurjchem-29 136 368 less less ADJ eurjchem-29 136 369     SPACE eurjchem-29 136 370 active active ADJ eurjchem-29 136 371 ) ) PUNCT eurjchem-29 136 372 ; ; PUNCT eurjchem-29 136 373     SPACE eurjchem-29 136 374 inhibition inhibition NOUN eurjchem-29 136 375     SPACE eurjchem-29 136 376 values value NOUN eurjchem-29 136 377     SPACE eurjchem-29 136 378 = = NOUN eurjchem-29 136 379     SPACE eurjchem-29 136 380 0.6–1.0 0.6–1.0 NOUN eurjchem-29 136 381     SPACE eurjchem-29 136 382 cm cm NOUN eurjchem-29 136 383     SPACE eurjchem-29 136 384 beyond beyond ADP eurjchem-29 136 385     SPACE eurjchem-29 136 386 control control NOUN eurjchem-29 136 387     SPACE eurjchem-29 137 1 = = NOUN eurjchem-29 137 2     SPACE eurjchem-29 137 3 + + ADJ eurjchem-29 137 4 + + NOUN eurjchem-29 137 5     SPACE eurjchem-29 137 6 ( ( PUNCT eurjchem-29 137 7 moderate moderate ADJ eurjchem-29 137 8     SPACE eurjchem-29 137 9 active active ADJ eurjchem-29 137 10 ) ) PUNCT eurjchem-29 137 11 ; ; PUNCT eurjchem-29 137 12     SPACE eurjchem-29 137 13 inhibition inhibition NOUN eurjchem-29 137 14     SPACE eurjchem-29 137 15 values value NOUN eurjchem-29 137 16     SPACE eurjchem-29 137 17 = = NOUN eurjchem-29 137 18 1.1–1.5 1.1–1.5 NOUN eurjchem-29 137 19     SPACE eurjchem-29 137 20 cm cm NOUN eurjchem-29 137 21     SPACE eurjchem-29 137 22 beyond beyond ADP eurjchem-29 137 23     SPACE eurjchem-29 137 24 control= control= NOUN eurjchem-29 137 25     SPACE eurjchem-29 138 1 + + PROPN eurjchem-29 138 2 + + ADJ eurjchem-29 138 3 + + NOUN eurjchem-29 138 4     SPACE eurjchem-29 138 5 ( ( PUNCT eurjchem-29 138 6 highly highly ADV eurjchem-29 138 7     SPACE eurjchem-29 138 8 active active ADJ eurjchem-29 138 9 ) ) PUNCT eurjchem-29 138 10 ; ; PUNCT eurjchem-29 138 11     SPACE eurjchem-29 138 12 solvent solvent NOUN eurjchem-29 138 13     SPACE eurjchem-29 138 14 control control NOUN eurjchem-29 138 15 : : PUNCT eurjchem-29 138 16     SPACE eurjchem-29 138 17 dmf dmf PROPN eurjchem-29 138 18     SPACE eurjchem-29 138 19 for for ADP eurjchem-29 138 20     SPACE eurjchem-29 138 21 antibacterial antibacterial ADJ eurjchem-29 138 22 ; ; PUNCT eurjchem-29 138 23     SPACE eurjchem-29 138 24 chloramphenicol chloramphenicol NOUN eurjchem-29 138 25     SPACE eurjchem-29 138 26 for for ADP eurjchem-29 138 27     SPACE eurjchem-29 138 28 antibacterial antibacterial ADJ eurjchem-29 138 29 : : PUNCT eurjchem-29 138 30     SPACE eurjchem-29 138 31 terbianfin terbianfin NOUN eurjchem-29 138 32     SPACE eurjchem-29 138 33 for for ADP eurjchem-29 138 34     SPACE eurjchem-29 138 35 antifungal antifungal PROPN eurjchem-29 138 36 . . PUNCT eurjchem-29 138 37           SPACE eurjchem-29 139 1 references reference NOUN eurjchem-29 139 2         SPACE eurjchem-29 139 3 [ [ X eurjchem-29 139 4 1 1 NUM eurjchem-29 139 5 ] ] PUNCT eurjchem-29 139 6 . . PUNCT eurjchem-29 140 1 el‐gendy el‐gendy PROPN eurjchem-29 140 2 , , PUNCT eurjchem-29 140 3     SPACE eurjchem-29 140 4 z. z. PROPN eurjchem-29 140 5 ; ; PUNCT eurjchem-29 140 6     SPACE eurjchem-29 140 7 morsy morsy NOUN eurjchem-29 140 8 , , PUNCT eurjchem-29 140 9     SPACE eurjchem-29 140 10 j. j. PROPN eurjchem-29 140 11     SPACE eurjchem-29 140 12 m. m. NOUN eurjchem-29 140 13 ; ; PUNCT eurjchem-29 140 14     SPACE eurjchem-29 140 15 allimony allimony ADJ eurjchem-29 140 16 , , PUNCT eurjchem-29 140 17     SPACE eurjchem-29 140 18 h. h. PROPN eurjchem-29 140 19     SPACE eurjchem-29 140 20 a a PROPN eurjchem-29 140 21 ; ; PUNCT eurjchem-29 140 22     SPACE eurjchem-29 140 23 abdel‐monem abdel‐monem PROPN eurjchem-29 140 24     SPACE eurjchem-29 140 25 ali ali PROPN eurjchem-29 140 26 , , PUNCT eurjchem-29 140 27     SPACE eurjchem-29 140 28 w. w. PROPN eurjchem-29 140 29     SPACE eurjchem-29 140 30 r. r. PROPN eurjchem-29 140 31 ; ; PUNCT eurjchem-29 140 32     SPACE eurjchem-29 140 33 abdel‐rahman abdel‐rahman NOUN eurjchem-29 140 34 , , PUNCT eurjchem-29 140 35     SPACE eurjchem-29 140 36 r. r. PROPN eurjchem-29 140 37     SPACE eurjchem-29 140 38 m. m. NOUN eurjchem-29 140 39     SPACE eurjchem-29 140 40 phosphorus phosphorus NOUN eurjchem-29 140 41 , , PUNCT eurjchem-29 140 42     SPACE eurjchem-29 140 43 sulfur sulfur NOUN eurjchem-29 140 44     SPACE eurjchem-29 140 45 silicon silicon NOUN eurjchem-29 140 46     SPACE eurjchem-29 140 47 relat relat NOUN eurjchem-29 140 48 . . PUNCT eurjchem-29 140 49     SPACE eurjchem-29 140 50 elem elem NOUN eurjchem-29 140 51 . . PUNCT eurjchem-29 140 52     SPACE eurjchem-29 140 53 2003 2003 NUM eurjchem-29 140 54 , , PUNCT eurjchem-29 140 55     SPACE eurjchem-29 140 56 178(9 178(9 NUM eurjchem-29 140 57 ) ) PUNCT eurjchem-29 140 58 , , PUNCT eurjchem-29 140 59     SPACE eurjchem-29 140 60 2055‐2071 2055‐2071 NUM eurjchem-29 140 61 . . PUNCT eurjchem-29 140 62     SPACE eurjchem-29 141 1 [ [ X eurjchem-29 141 2 2 2 NUM eurjchem-29 141 3 ] ] PUNCT eurjchem-29 141 4 . . PUNCT eurjchem-29 142 1 erickson erickson PROPN eurjchem-29 142 2 , , PUNCT eurjchem-29 142 3     SPACE eurjchem-29 142 4 j. j. PROPN eurjchem-29 142 5     SPACE eurjchem-29 142 6 g. g. PROPN eurjchem-29 142 7     SPACE eurjchem-29 142 8 chem chem NOUN eurjchem-29 142 9 . . PUNCT eurjchem-29 142 10     SPACE eurjchem-29 142 11 heterocycl heterocycl PROPN eurjchem-29 142 12 . . PUNCT eurjchem-29 142 13     SPACE eurjchem-29 142 14 compd compd NOUN eurjchem-29 142 15 . . PUNCT eurjchem-29 142 16     SPACE eurjchem-29 142 17 1956 1956 NUM eurjchem-29 142 18 , , PUNCT eurjchem-29 142 19     SPACE eurjchem-29 142 20 10 10 NUM eurjchem-29 142 21 , , PUNCT eurjchem-29 142 22     SPACE eurjchem-29 142 23 44‐51 44‐51 NOUN eurjchem-29 142 24 . . PUNCT eurjchem-29 142 25     SPACE eurjchem-29 143 1 [ [ X eurjchem-29 143 2 3 3 NUM eurjchem-29 143 3 ] ] PUNCT eurjchem-29 143 4 . . PUNCT eurjchem-29 144 1 jones jones PROPN eurjchem-29 144 2 , , PUNCT eurjchem-29 144 3     SPACE eurjchem-29 144 4 r. r. PROPN eurjchem-29 144 5     SPACE eurjchem-29 144 6 l. l. PROPN eurjchem-29 144 7 ; ; PUNCT eurjchem-29 144 8     SPACE eurjchem-29 144 9 kershaw kershaw PROPN eurjchem-29 144 10 , , PUNCT eurjchem-29 144 11     SPACE eurjchem-29 144 12 j. j. PROPN eurjchem-29 144 13     SPACE eurjchem-29 144 14 r. r. PROPN eurjchem-29 144 15     SPACE eurjchem-29 144 16 rev rev PROPN eurjchem-29 144 17 . . PROPN eurjchem-29 144 18     SPACE eurjchem-29 144 19 pure pure ADJ eurjchem-29 144 20     SPACE eurjchem-29 144 21 appl appl NOUN eurjchem-29 144 22 . . PUNCT eurjchem-29 144 23     SPACE eurjchem-29 144 24 chem chem NOUN eurjchem-29 144 25 . . PUNCT eurjchem-29 144 26     SPACE eurjchem-29 144 27 1971 1971 NUM eurjchem-29 144 28 , , PUNCT eurjchem-29 144 29     SPACE eurjchem-29 144 30 21 21 NUM eurjchem-29 144 31 , , PUNCT eurjchem-29 144 32     SPACE eurjchem-29 144 33 23‐29 23‐29 NUM eurjchem-29 144 34 . . PUNCT eurjchem-29 144 35     SPACE eurjchem-29 145 1 [ [ X eurjchem-29 145 2 4 4 NUM eurjchem-29 145 3 ] ] PUNCT eurjchem-29 145 4 . . PUNCT eurjchem-29 145 5     SPACE eurjchem-29 145 6 neunhoeffer neunhoeffer NOUN eurjchem-29 145 7 , , PUNCT eurjchem-29 145 8     SPACE eurjchem-29 145 9 h. h. PROPN eurjchem-29 145 10 ; ; PUNCT eurjchem-29 145 11     SPACE eurjchem-29 145 12 wiley wiley NOUN eurjchem-29 145 13 , , PUNCT eurjchem-29 145 14     SPACE eurjchem-29 145 15 p. p. NOUN eurjchem-29 145 16     SPACE eurjchem-29 145 17 f. f. PROPN eurjchem-29 145 18     SPACE eurjchem-29 145 19 chem chem NOUN eurjchem-29 145 20 . . PUNCT eurjchem-29 145 21     SPACE eurjchem-29 145 22 heterocycl heterocycl PROPN eurjchem-29 145 23 . . PUNCT eurjchem-29 145 24     SPACE eurjchem-29 146 1 compd compd NOUN eurjchem-29 146 2 . . PUNCT eurjchem-29 146 3     SPACE eurjchem-29 147 1 1978 1978 NUM eurjchem-29 147 2 , , PUNCT eurjchem-29 147 3     SPACE eurjchem-29 147 4 33 33 NUM eurjchem-29 147 5 , , PUNCT eurjchem-29 147 6     SPACE eurjchem-29 147 7 189‐ 189‐ NUM eurjchem-29 147 8 196 196 NUM eurjchem-29 147 9 . . PUNCT eurjchem-29 147 10     SPACE eurjchem-29 148 1 [ [ X eurjchem-29 148 2 5 5 NUM eurjchem-29 148 3 ] ] PUNCT eurjchem-29 148 4 . . PUNCT eurjchem-29 148 5     SPACE eurjchem-29 149 1 el el PROPN eurjchem-29 149 2     SPACE eurjchem-29 149 3 ashry ashry ADJ eurjchem-29 149 4 , , PUNCT eurjchem-29 149 5     SPACE eurjchem-29 149 6 e. e. PROPN eurjchem-29 149 7     SPACE eurjchem-29 149 8 h. h. PROPN eurjchem-29 149 9 ; ; PUNCT eurjchem-29 149 10     SPACE eurjchem-29 149 11 rashed rashe VERB eurjchem-29 149 12 , , PUNCT eurjchem-29 149 13     SPACE eurjchem-29 149 14 m. m. NOUN eurjchem-29 149 15 ; ; PUNCT eurjchem-29 149 16     SPACE eurjchem-29 149 17 taha taha NOUN eurjchem-29 149 18 , , PUNCT eurjchem-29 149 19     SPACE eurjchem-29 149 20 e. e. PROPN eurjchem-29 149 21 ; ; PUNCT eurjchem-29 149 22     SPACE eurjchem-29 149 23 ramadan ramadan PROPN eurjchem-29 149 24 , , PUNCT eurjchem-29 149 25     SPACE eurjchem-29 149 26 e. e. PROPN eurjchem-29 149 27     SPACE eurjchem-29 149 28 adv adv PROPN eurjchem-29 149 29 . . PUNCT eurjchem-29 149 30     SPACE eurjchem-29 149 31 heterocycl heterocycl PROPN eurjchem-29 149 32 . . PUNCT eurjchem-29 149 33     SPACE eurjchem-29 149 34 chem chem NOUN eurjchem-29 149 35 . . PUNCT eurjchem-29 149 36     SPACE eurjchem-29 149 37 1994 1994 NUM eurjchem-29 149 38 , , PUNCT eurjchem-29 149 39     SPACE eurjchem-29 149 40 59 59 NUM eurjchem-29 149 41 , , PUNCT eurjchem-29 149 42     SPACE eurjchem-29 149 43 39‐46 39‐46 NUM eurjchem-29 149 44 . . PUNCT eurjchem-29 149 45     SPACE eurjchem-29 150 1 [ [ X eurjchem-29 150 2 6 6 NUM eurjchem-29 150 3 ] ] PUNCT eurjchem-29 150 4 . . PUNCT eurjchem-29 150 5     SPACE eurjchem-29 150 6 abdel‐rahman abdel‐rahman NOUN eurjchem-29 150 7 , , PUNCT eurjchem-29 150 8     SPACE eurjchem-29 150 9 r. r. NOUN eurjchem-29 150 10     SPACE eurjchem-29 150 11 m. m. NOUN eurjchem-29 150 12     SPACE eurjchem-29 150 13 pharmazie pharmazie PROPN eurjchem-29 150 14     SPACE eurjchem-29 150 15 2001 2001 NUM eurjchem-29 150 16 , , PUNCT eurjchem-29 150 17     SPACE eurjchem-29 150 18 56 56 NUM eurjchem-29 150 19 , , PUNCT eurjchem-29 150 20     SPACE eurjchem-29 150 21 275‐281 275‐281 NOUN eurjchem-29 150 22 . . PUNCT eurjchem-29 150 23     SPACE eurjchem-29 151 1 [ [ X eurjchem-29 151 2 7 7 NUM eurjchem-29 151 3 ] ] PUNCT eurjchem-29 151 4 . . PUNCT eurjchem-29 151 5     SPACE eurjchem-29 151 6 el‐gendy el‐gendy ADJ eurjchem-29 151 7 , , PUNCT eurjchem-29 151 8     SPACE eurjchem-29 151 9 z. z. PROPN eurjchem-29 151 10 ; ; PUNCT eurjchem-29 151 11     SPACE eurjchem-29 151 12 morsy morsy NOUN eurjchem-29 151 13 , , PUNCT eurjchem-29 151 14     SPACE eurjchem-29 151 15 j. j. PROPN eurjchem-29 151 16     SPACE eurjchem-29 151 17 m. m. NOUN eurjchem-29 151 18 ; ; PUNCT eurjchem-29 151 19     SPACE eurjchem-29 151 20 allimony allimony ADJ eurjchem-29 151 21 , , PUNCT eurjchem-29 151 22     SPACE eurjchem-29 151 23 h. h. PROPN eurjchem-29 151 24     SPACE eurjchem-29 151 25 m. m. NOUN eurjchem-29 151 26 ; ; PUNCT eurjchem-29 151 27     SPACE eurjchem-29 151 28 abdel‐monem abdel‐monem PROPN eurjchem-29 151 29     SPACE eurjchem-29 151 30 ali ali PROPN eurjchem-29 151 31 , , PUNCT eurjchem-29 151 32     SPACE eurjchem-29 151 33 w. w. PROPN eurjchem-29 151 34     SPACE eurjchem-29 151 35 r. r. PROPN eurjchem-29 151 36 ; ; PUNCT eurjchem-29 151 37     SPACE eurjchem-29 151 38 abdel‐rahman abdel‐rahman NOUN eurjchem-29 151 39 , , PUNCT eurjchem-29 151 40     SPACE eurjchem-29 151 41 r. r. NOUN eurjchem-29 151 42     SPACE eurjchem-29 151 43 m. m. NOUN eurjchem-29 151 44     SPACE eurjchem-29 151 45 pharmazie pharmazie PROPN eurjchem-29 151 46     SPACE eurjchem-29 151 47 2001 2001 NUM eurjchem-29 151 48 , , PUNCT eurjchem-29 151 49     SPACE eurjchem-29 151 50 56 56 NUM eurjchem-29 151 51 , , PUNCT eurjchem-29 151 52     SPACE eurjchem-29 151 53 376‐381 376‐381 NUM eurjchem-29 151 54 . . PUNCT eurjchem-29 151 55     SPACE eurjchem-29 152 1 [ [ X eurjchem-29 152 2 8 8 NUM eurjchem-29 152 3 ] ] PUNCT eurjchem-29 152 4 . . PUNCT eurjchem-29 152 5     SPACE eurjchem-29 152 6 hunt hunt NOUN eurjchem-29 152 7 , , PUNCT eurjchem-29 152 8     SPACE eurjchem-29 152 9 j. j. PROPN eurjchem-29 152 10     SPACE eurjchem-29 152 11 t. t. PROPN eurjchem-29 152 12 ; ; PUNCT eurjchem-29 152 13     SPACE eurjchem-29 152 14 mitt mitt PROPN eurjchem-29 152 15 , , PUNCT eurjchem-29 152 16     SPACE eurjchem-29 152 17 t. t. PROPN eurjchem-29 152 18 ; ; PUNCT eurjchem-29 152 19     SPACE eurjchem-29 152 20 borzilleri borzilleri PROPN eurjchem-29 152 21 , , PUNCT eurjchem-29 152 22     SPACE eurjchem-29 152 23 r. r. PROPN eurjchem-29 152 24 ; ; PUNCT eurjchem-29 152 25     SPACE eurjchem-29 152 26 brown brown ADJ eurjchem-29 152 27 , , PUNCT eurjchem-29 152 28     SPACE eurjchem-29 152 29 j. j. PROPN eurjchem-29 152 30 ; ; PUNCT eurjchem-29 152 31     SPACE eurjchem-29 152 32 fink fink VERB eurjchem-29 152 33 , , PUNCT eurjchem-29 152 34     SPACE eurjchem-29 152 35 b. b. PROPN eurjchem-29 152 36 ; ; PUNCT eurjchem-29 152 37     SPACE eurjchem-29 152 38 bhide bhide NOUN eurjchem-29 152 39 . . PUNCT eurjchem-29 152 40     SPACE eurjchem-29 152 41 j. j. PROPN eurjchem-29 152 42     SPACE eurjchem-29 152 43 med med PROPN eurjchem-29 152 44 . . PUNCT eurjchem-29 152 45     SPACE eurjchem-29 152 46 chem chem NOUN eurjchem-29 152 47 . . PUNCT eurjchem-29 152 48     SPACE eurjchem-29 152 49 2007 2007 NUM eurjchem-29 152 50 , , PUNCT eurjchem-29 152 51     SPACE eurjchem-29 152 52 47 47 NUM eurjchem-29 152 53 , , PUNCT eurjchem-29 152 54     SPACE eurjchem-29 152 55 4054‐4059 4054‐4059 NUM eurjchem-29 152 56 . . PUNCT eurjchem-29 152 57     SPACE eurjchem-29 153 1 [ [ X eurjchem-29 153 2 9 9 NUM eurjchem-29 153 3 ] ] PUNCT eurjchem-29 153 4 . . PUNCT eurjchem-29 153 5     SPACE eurjchem-29 153 6 sztanke sztanke NOUN eurjchem-29 153 7 , , PUNCT eurjchem-29 153 8     SPACE eurjchem-29 153 9 k. k. PROPN eurjchem-29 153 10 ; ; PUNCT eurjchem-29 153 11     SPACE eurjchem-29 153 12 rzmowska rzmowska NOUN eurjchem-29 153 13 , , PUNCT eurjchem-29 153 14     SPACE eurjchem-29 153 15 j. j. PROPN eurjchem-29 153 16 ; ; PUNCT eurjchem-29 153 17     SPACE eurjchem-29 153 18 niemczyk niemczyk NOUN eurjchem-29 153 19 , , PUNCT eurjchem-29 153 20     SPACE eurjchem-29 153 21 m. m. NOUN eurjchem-29 153 22 ; ; PUNCT eurjchem-29 153 23     SPACE eurjchem-29 153 24 dybala dybala NOUN eurjchem-29 153 25 , , PUNCT eurjchem-29 153 26     SPACE eurjchem-29 153 27 i. i. NOUN eurjchem-29 153 28 ; ; PUNCT eurjchem-29 153 29     SPACE eurjchem-29 153 30 koizoi koizoi NOUN eurjchem-29 153 31 , , PUNCT eurjchem-29 153 32         SPACE eurjchem-29 153 33 a. a. NOUN eurjchem-29 153 34     SPACE eurjchem-29 153 35 eur eur PROPN eurjchem-29 153 36 . . PUNCT eurjchem-29 153 37     SPACE eurjchem-29 153 38 med med ADJ eurjchem-29 153 39 . . PUNCT eurjchem-29 153 40     SPACE eurjchem-29 153 41 chem chem NOUN eurjchem-29 153 42 . . PUNCT eurjchem-29 153 43     SPACE eurjchem-29 154 1 2006 2006 NUM eurjchem-29 154 2 , , PUNCT eurjchem-29 154 3     SPACE eurjchem-29 154 4 41 41 NUM eurjchem-29 154 5 , , PUNCT eurjchem-29 154 6     SPACE eurjchem-29 154 7 1373‐1379 1373‐1379 NUM eurjchem-29 154 8 . . PUNCT eurjchem-29 154 9     SPACE eurjchem-29 155 1 [ [ X eurjchem-29 155 2 10 10 NUM eurjchem-29 155 3 ] ] PUNCT eurjchem-29 155 4 . . PUNCT eurjchem-29 155 5     SPACE eurjchem-29 155 6 sarvesh sarvesh PROPN eurjchem-29 155 7     SPACE eurjchem-29 155 8 kumar kumar PROPN eurjchem-29 155 9 , , PUNCT eurjchem-29 155 10     SPACE eurjchem-29 155 11 p. p. NOUN eurjchem-29 155 12 ; ; PUNCT eurjchem-29 155 13     SPACE eurjchem-29 155 14 abhishek abhishek NOUN eurjchem-29 155 15 , , PUNCT eurjchem-29 155 16     SPACE eurjchem-29 155 17 f. f. PROPN eurjchem-29 155 18 ; ; PUNCT eurjchem-29 155 19     SPACE eurjchem-29 155 20 ashutash ashutash NOUN eurjchem-29 155 21 , , PUNCT eurjchem-29 155 22     SPACE eurjchem-29 155 23 s. s. PROPN eurjchem-29 155 24 ; ; PUNCT eurjchem-29 155 25     SPACE eurjchem-29 155 26 nizamuddin nizamuddin ADV eurjchem-29 155 27 , , PUNCT eurjchem-29 155 28     SPACE eurjchem-29 155 29 s. s. PROPN eurjchem-29 155 30     SPACE eurjchem-29 155 31 j. j. PROPN eurjchem-29 155 32     SPACE eurjchem-29 155 33 eur eur PROPN eurjchem-29 155 34 . . PUNCT eurjchem-29 155 35     SPACE eurjchem-29 155 36 med med ADJ eurjchem-29 155 37 . . PUNCT eurjchem-29 155 38     SPACE eurjchem-29 155 39 chem chem NOUN eurjchem-29 155 40 . . PUNCT eurjchem-29 155 41       SPACE eurjchem-29 156 1 2009 2009 NUM eurjchem-29 156 2 , , PUNCT eurjchem-29 156 3     SPACE eurjchem-29 156 4 44 44 NUM eurjchem-29 156 5 , , PUNCT eurjchem-29 156 6     SPACE eurjchem-29 156 7 1188‐1196 1188‐1196 NUM eurjchem-29 156 8 . . PUNCT eurjchem-29 156 9     SPACE eurjchem-29 157 1 [ [ X eurjchem-29 157 2 11 11 NUM eurjchem-29 157 3 ] ] PUNCT eurjchem-29 157 4 . . PUNCT eurjchem-29 157 5     SPACE eurjchem-29 157 6 deeb deeb PROPN eurjchem-29 157 7 , , PUNCT eurjchem-29 157 8     SPACE eurjchem-29 157 9 a. a. NOUN eurjchem-29 157 10 ; ; PUNCT eurjchem-29 157 11     SPACE eurjchem-29 157 12 el­mariah el­mariah PROPN eurjchem-29 157 13 , , PUNCT eurjchem-29 157 14     SPACE eurjchem-29 157 15 f. f. PROPN eurjchem-29 157 16 ; ; PUNCT eurjchem-29 157 17     SPACE eurjchem-29 157 18 hosny hosny PROPN eurjchem-29 157 19 , , PUNCT eurjchem-29 157 20     SPACE eurjchem-29 157 21 m. m. NOUN eurjchem-29 157 22     SPACE eurjchem-29 157 23 a. a. NOUN eurjchem-29 157 24     SPACE eurjchem-29 157 25 bioorg bioorg PROPN eurjchem-29 157 26 . . PUNCT eurjchem-29 157 27     SPACE eurjchem-29 157 28 med med PROPN eurjchem-29 157 29 . . PUNCT eurjchem-29 157 30     SPACE eurjchem-29 157 31 chem chem NOUN eurjchem-29 157 32 . . PUNCT eurjchem-29 157 33     SPACE eurjchem-29 158 1 lett lett PROPN eurjchem-29 158 2 . . PUNCT eurjchem-29 158 3     SPACE eurjchem-29 159 1 2004 2004 NUM eurjchem-29 159 2 , , PUNCT eurjchem-29 159 3     SPACE eurjchem-29 159 4 14 14 NUM eurjchem-29 159 5 , , PUNCT eurjchem-29 159 6     SPACE eurjchem-29 159 7 5013‐5017 5013‐5017 NUM eurjchem-29 159 8 . . PUNCT eurjchem-29 159 9     SPACE eurjchem-29 160 1 [ [ X eurjchem-29 160 2 12 12 NUM eurjchem-29 160 3 ] ] PUNCT eurjchem-29 160 4 . . PUNCT eurjchem-29 160 5     SPACE eurjchem-29 160 6 cai cai X eurjchem-29 160 7 , , PUNCT eurjchem-29 160 8     SPACE eurjchem-29 160 9 s. s. PROPN eurjchem-29 160 10 ; ; PUNCT eurjchem-29 160 11     SPACE eurjchem-29 160 12 li li PROPN eurjchem-29 160 13 , , PUNCT eurjchem-29 160 14     SPACE eurjchem-29 160 15 q. q. PROPN eurjchem-29 160 16     SPACE eurjchem-29 160 17 s. s. PROPN eurjchem-29 160 18 ; ; PUNCT eurjchem-29 160 19     SPACE eurjchem-29 160 20 borchardt borchardt ADJ eurjchem-29 160 21 , , PUNCT eurjchem-29 160 22     SPACE eurjchem-29 160 23 r. r. PROPN eurjchem-29 160 24     SPACE eurjchem-29 160 25 t. t. PROPN eurjchem-29 160 26 ; ; PUNCT eurjchem-29 160 27     SPACE eurjchem-29 160 28 kuczera kuczera NOUN eurjchem-29 160 29 , , PUNCT eurjchem-29 160 30     SPACE eurjchem-29 160 31 k. k. PROPN eurjchem-29 160 32 ; ; PUNCT eurjchem-29 160 33     SPACE eurjchem-29 160 34 schowen schowen NOUN eurjchem-29 160 35 , , PUNCT eurjchem-29 160 36     SPACE eurjchem-29 160 37 r. r. PROPN eurjchem-29 160 38     SPACE eurjchem-29 160 39 l. l. PROPN eurjchem-29 160 40     SPACE eurjchem-29 160 41 bioorg bioorg PROPN eurjchem-29 160 42 . . PUNCT eurjchem-29 160 43     SPACE eurjchem-29 160 44 med med ADJ eurjchem-29 160 45 . . PUNCT eurjchem-29 160 46     SPACE eurjchem-29 160 47 chem chem NOUN eurjchem-29 160 48 . . PUNCT eurjchem-29 160 49     SPACE eurjchem-29 161 1 2007 2007 NUM eurjchem-29 161 2 , , PUNCT eurjchem-29 161 3     SPACE eurjchem-29 161 4 15 15 NUM eurjchem-29 161 5 , , PUNCT eurjchem-29 161 6     SPACE eurjchem-29 161 7 7281‐7287 7281‐7287 NUM eurjchem-29 161 8 . . PUNCT eurjchem-29 161 9     SPACE eurjchem-29 162 1 [ [ X eurjchem-29 162 2 13 13 NUM eurjchem-29 162 3 ] ] PUNCT eurjchem-29 162 4 . . PUNCT eurjchem-29 162 5     SPACE eurjchem-29 162 6 demirbas demirbas NOUN eurjchem-29 162 7 , , PUNCT eurjchem-29 162 8     SPACE eurjchem-29 162 9 a. a. NOUN eurjchem-29 162 10 ; ; PUNCT eurjchem-29 162 11     SPACE eurjchem-29 162 12 ceylan ceylan NOUN eurjchem-29 162 13 , , PUNCT eurjchem-29 162 14     SPACE eurjchem-29 162 15 s. s. PROPN eurjchem-29 162 16 ; ; PUNCT eurjchem-29 162 17     SPACE eurjchem-29 162 18 demirbas demirbas NOUN eurjchem-29 162 19 , , PUNCT eurjchem-29 162 20     SPACE eurjchem-29 162 21 n. n. PROPN eurjchem-29 162 22     SPACE eurjchem-29 162 23 j. j. PROPN eurjchem-29 162 24     SPACE eurjchem-29 162 25 heterocycl heterocycl PROPN eurjchem-29 162 26 . . PUNCT eurjchem-29 162 27     SPACE eurjchem-29 162 28 chem chem NOUN eurjchem-29 162 29 . . PUNCT eurjchem-29 162 30     SPACE eurjchem-29 162 31 2007 2007 NUM eurjchem-29 162 32 , , PUNCT eurjchem-29 162 33     SPACE eurjchem-29 162 34 44 44 NUM eurjchem-29 162 35 , , PUNCT eurjchem-29 162 36     SPACE eurjchem-29 162 37 1271‐1280 1271‐1280 NUM eurjchem-29 162 38 . . PUNCT eurjchem-29 162 39     SPACE eurjchem-29 163 1 [ [ X eurjchem-29 163 2 14 14 NUM eurjchem-29 163 3 ] ] PUNCT eurjchem-29 163 4 . . PUNCT eurjchem-29 163 5     SPACE eurjchem-29 163 6 gewald gewald NOUN eurjchem-29 163 7 , , PUNCT eurjchem-29 163 8     SPACE eurjchem-29 163 9 k. k. PROPN eurjchem-29 163 10     SPACE eurjchem-29 163 11 g. g. PROPN eurjchem-29 163 12 ; ; PUNCT eurjchem-29 163 13     SPACE eurjchem-29 163 14 schnbelt schnbelt ADJ eurjchem-29 163 15 , , PUNCT eurjchem-29 163 16     SPACE eurjchem-29 163 17 a. a. NOUN eurjchem-29 163 18 ; ; PUNCT eurjchem-29 163 19     SPACE eurjchem-29 163 20 martin martin PROPN eurjchem-29 163 21 , , PUNCT eurjchem-29 163 22     SPACE eurjchem-29 163 23 g. g. PROPN eurjchem-29 163 24     SPACE eurjchem-29 163 25 j. j. PROPN eurjchem-29 163 26     SPACE eurjchem-29 163 27 prakt prakt NOUN eurjchem-29 163 28 . . PUNCT eurjchem-29 163 29     SPACE eurjchem-29 163 30 chem chem NOUN eurjchem-29 163 31 . . PUNCT eurjchem-29 163 32     SPACE eurjchem-29 163 33 1975 1975 NUM eurjchem-29 163 34 , , PUNCT eurjchem-29 163 35     SPACE eurjchem-29 163 36 317 317 NUM eurjchem-29 163 37 , , PUNCT eurjchem-29 163 38     SPACE eurjchem-29 163 39 561‐ 561‐ NUM eurjchem-29 163 40 569 569 NUM eurjchem-29 163 41 . . PUNCT eurjchem-29 163 42     SPACE eurjchem-29 164 1 [ [ X eurjchem-29 164 2 15 15 NUM eurjchem-29 164 3 ] ] PUNCT eurjchem-29 164 4 . . PUNCT eurjchem-29 164 5     SPACE eurjchem-29 164 6 al‐omran al‐omran PROPN eurjchem-29 164 7 , , PUNCT eurjchem-29 164 8     SPACE eurjchem-29 164 9 f. f. PROPN eurjchem-29 164 10 ; ; PUNCT eurjchem-29 164 11     SPACE eurjchem-29 164 12 abdel abdel PROPN eurjchem-29 164 13     SPACE eurjchem-29 164 14 khalik khalik PROPN eurjchem-29 164 15     SPACE eurjchem-29 164 16 m. m. NOUN eurjchem-29 164 17 ; ; PUNCT eurjchem-29 164 18     SPACE eurjchem-29 164 19 elna elna PROPN eurjchem-29 164 20 , , PUNCT eurjchem-29 164 21     SPACE eurjchem-29 164 22 m. m. NOUN eurjchem-29 164 23     SPACE eurjchem-29 164 24 h. h. PROPN eurjchem-29 164 25     SPACE eurjchem-29 164 26 j. j. PROPN eurjchem-29 164 27     SPACE eurjchem-29 164 28 heterocycl heterocycl PROPN eurjchem-29 164 29 . . PUNCT eurjchem-29 164 30     SPACE eurjchem-29 165 1 chem chem NOUN eurjchem-29 165 2 . . PUNCT eurjchem-29 165 3     SPACE eurjchem-29 166 1 1995 1995 NUM eurjchem-29 166 2 , , PUNCT eurjchem-29 166 3     SPACE eurjchem-29 166 4 6 6 NUM eurjchem-29 166 5 , , PUNCT eurjchem-29 166 6     SPACE eurjchem-29 166 7 545‐564 545‐564 NUM eurjchem-29 166 8 . . PUNCT eurjchem-29 166 9     SPACE eurjchem-29 167 1 [ [ X eurjchem-29 167 2 16 16 NUM eurjchem-29 167 3 ] ] PUNCT eurjchem-29 167 4 . . PUNCT eurjchem-29 167 5     SPACE eurjchem-29 167 6 abdel‐monem abdel‐monem PROPN eurjchem-29 167 7 , , PUNCT eurjchem-29 167 8     SPACE eurjchem-29 167 9 w. w. PROPN eurjchem-29 167 10     SPACE eurjchem-29 167 11 r. r. PROPN eurjchem-29 167 12     SPACE eurjchem-29 167 13 chem chem NOUN eurjchem-29 167 14 . . PUNCT eurjchem-29 167 15     SPACE eurjchem-29 168 1 pap pap NOUN eurjchem-29 168 2 . . PUNCT eurjchem-29 168 3     SPACE eurjchem-29 168 4 2004 2004 NUM eurjchem-29 168 5 , , PUNCT eurjchem-29 168 6     SPACE eurjchem-29 168 7 276‐282 276‐282 NUM eurjchem-29 168 8 . . PUNCT eurjchem-29 168 9     SPACE eurjchem-29 169 1 [ [ X eurjchem-29 169 2 17 17 NUM eurjchem-29 169 3 ] ] PUNCT eurjchem-29 169 4 . . PUNCT eurjchem-29 169 5     SPACE eurjchem-29 169 6 abdel‐monem abdel‐monem PROPN eurjchem-29 169 7 , , PUNCT eurjchem-29 169 8     SPACE eurjchem-29 169 9 w. w. PROPN eurjchem-29 169 10     SPACE eurjchem-29 169 11 r. r. PROPN eurjchem-29 169 12       SPACE eurjchem-29 169 13 boll boll NOUN eurjchem-29 169 14 . . PUNCT eurjchem-29 169 15     SPACE eurjchem-29 170 1 chim chim PROPN eurjchem-29 170 2 . . PUNCT eurjchem-29 170 3     SPACE eurjchem-29 171 1 farmaco farmaco PROPN eurjchem-29 171 2 , , PUNCT eurjchem-29 171 3     SPACE eurjchem-29 171 4 2004 2004 NUM eurjchem-29 171 5 , , PUNCT eurjchem-29 171 6     SPACE eurjchem-29 171 7 143(6 143(6 NUM eurjchem-29 171 8 ) ) PUNCT eurjchem-29 171 9 , , PUNCT eurjchem-29 171 10     SPACE eurjchem-29 171 11 239‐247 239‐247 PROPN eurjchem-29 171 12 . . PUNCT eurjchem-29 171 13     SPACE eurjchem-29 172 1 [ [ X eurjchem-29 172 2 18 18 NUM eurjchem-29 172 3 ] ] PUNCT eurjchem-29 172 4 . . PUNCT eurjchem-29 172 5     SPACE eurjchem-29 172 6 abdel‐monem abdel‐monem PROPN eurjchem-29 172 7 , , PUNCT eurjchem-29 172 8     SPACE eurjchem-29 172 9 w. w. PROPN eurjchem-29 172 10     SPACE eurjchem-29 172 11 r. r. PROPN eurjchem-29 172 12       SPACE eurjchem-29 172 13 boll boll NOUN eurjchem-29 172 14 . . PUNCT eurjchem-29 172 15     SPACE eurjchem-29 173 1 chim chim PROPN eurjchem-29 173 2 . . PUNCT eurjchem-29 173 3     SPACE eurjchem-29 174 1 farmaco farmaco PROPN eurjchem-29 174 2 , , PUNCT eurjchem-29 174 3     SPACE eurjchem-29 174 4 2005 2005 NUM eurjchem-29 174 5 , , PUNCT eurjchem-29 174 6     SPACE eurjchem-29 174 7 144(5 144(5 NUM eurjchem-29 174 8 ) ) PUNCT eurjchem-29 174 9 , , PUNCT eurjchem-29 174 10     SPACE eurjchem-29 174 11 1‐23 1‐23 NUM eurjchem-29 174 12 . . PUNCT eurjchem-29 174 13     SPACE eurjchem-29 175 1 [ [ X eurjchem-29 175 2 19 19 NUM eurjchem-29 175 3 ] ] PUNCT eurjchem-29 175 4 . . PUNCT eurjchem-29 175 5     SPACE eurjchem-29 175 6 abdel‐monem abdel‐monem PROPN eurjchem-29 175 7 , , PUNCT eurjchem-29 175 8     SPACE eurjchem-29 175 9 w. w. PROPN eurjchem-29 175 10     SPACE eurjchem-29 175 11 r. r. PROPN eurjchem-29 175 12 ; ; PUNCT eurjchem-29 175 13     SPACE eurjchem-29 175 14 ali ali PROPN eurjchem-29 175 15 , , PUNCT eurjchem-29 175 16     SPACE eurjchem-29 175 17 t. t. PROPN eurjchem-29 175 18     SPACE eurjchem-29 175 19 e. e. PROPN eurjchem-29 175 20       SPACE eurjchem-29 175 21 int int PROPN eurjchem-29 175 22 . . PUNCT eurjchem-29 175 23     SPACE eurjchem-29 175 24 j. j. PROPN eurjchem-29 175 25     SPACE eurjchem-29 175 26 chem chem NOUN eurjchem-29 175 27 . . PUNCT eurjchem-29 175 28     SPACE eurjchem-29 176 1 2007 2007 NUM eurjchem-29 176 2 , , PUNCT eurjchem-29 176 3     SPACE eurjchem-29 176 4 17 17 NUM eurjchem-29 176 5 , , PUNCT eurjchem-29 176 6     SPACE eurjchem-29 176 7 303‐314 303‐314 NOUN eurjchem-29 176 8 . . PUNCT eurjchem-29 176 9     SPACE eurjchem-29 177 1 [ [ X eurjchem-29 177 2 20 20 NUM eurjchem-29 177 3 ] ] PUNCT eurjchem-29 177 4 . . PUNCT eurjchem-29 177 5     SPACE eurjchem-29 177 6 al‐najjar al‐najjar PROPN eurjchem-29 177 7 , , PUNCT eurjchem-29 177 8     SPACE eurjchem-29 177 9 a. a. NOUN eurjchem-29 177 10     SPACE eurjchem-29 177 11 a. a. NOUN eurjchem-29 177 12     SPACE eurjchem-29 177 13 a. a. NOUN eurjchem-29 177 14 ; ; PUNCT eurjchem-29 177 15     SPACE eurjchem-29 177 16 amer amer PROPN eurjchem-29 177 17 , , PUNCT eurjchem-29 177 18     SPACE eurjchem-29 177 19 s. s. PROPN eurjchem-29 177 20     SPACE eurjchem-29 177 21 a. a. NOUN eurjchem-29 177 22 ; ; PUNCT eurjchem-29 177 23     SPACE eurjchem-29 177 24 riad riad PROPN eurjchem-29 177 25 , , PUNCT eurjchem-29 177 26     SPACE eurjchem-29 177 27 m. m. NOUN eurjchem-29 177 28 ; ; PUNCT eurjchem-29 177 29     SPACE eurjchem-29 177 30 elghamy elghamy ADJ eurjchem-29 177 31 , , PUNCT eurjchem-29 177 32     SPACE eurjchem-29 177 33 i. i. NOUN eurjchem-29 177 34 ; ; PUNCT eurjchem-29 177 35     SPACE eurjchem-29 177 36 m. m. NOUN eurjchem-29 177 37     SPACE eurjchem-29 177 38 h. h. PROPN eurjchem-29 177 39     SPACE eurjchem-29 177 40 elnagdy elnagdy NOUN eurjchem-29 177 41 , , PUNCT eurjchem-29 177 42     SPACE eurjchem-29 177 43 m. m. NOUN eurjchem-29 177 44     SPACE eurjchem-29 177 45 h. h. PROPN eurjchem-29 177 46       SPACE eurjchem-29 177 47 j. j. PROPN eurjchem-29 177 48 chem chem PROPN eurjchem-29 177 49 . . PUNCT eurjchem-29 177 50     SPACE eurjchem-29 177 51 research research NOUN eurjchem-29 177 52     SPACE eurjchem-29 177 53 ( ( PUNCT eurjchem-29 177 54 s s NOUN eurjchem-29 177 55 ) ) PUNCT eurjchem-29 177 56 , , PUNCT eurjchem-29 177 57     SPACE eurjchem-29 177 58 1996 1996 NUM eurjchem-29 177 59 , , PUNCT eurjchem-29 177 60     SPACE eurjchem-29 177 61 296‐297 296‐297 PROPN eurjchem-29 177 62 . . PUNCT eurjchem-29 177 63     SPACE eurjchem-29 178 1 [ [ X eurjchem-29 178 2 21 21 NUM eurjchem-29 178 3 ] ] PUNCT eurjchem-29 178 4 . . PUNCT eurjchem-29 178 5     SPACE eurjchem-29 178 6 gould gould PROPN eurjchem-29 178 7 , , PUNCT eurjchem-29 178 8     SPACE eurjchem-29 178 9 j. j. PROPN eurjchem-29 178 10     SPACE eurjchem-29 178 11 c. c. PROPN eurjchem-29 178 12 ; ; PUNCT eurjchem-29 178 13     SPACE eurjchem-29 178 14 bowi bowi NOUN eurjchem-29 178 15 , , PUNCT eurjchem-29 178 16     SPACE eurjchem-29 178 17 j. j. PROPN eurjchem-29 178 18     SPACE eurjchem-29 178 19 m. m. PROPN eurjchem-29 178 20       SPACE eurjchem-29 178 21 j. j. PROPN eurjchem-29 178 22     SPACE eurjchem-29 178 23 eur eur PROPN eurjchem-29 178 24 . . PUNCT eurjchem-29 178 25     SPACE eurjchem-29 178 26 med med PROPN eurjchem-29 178 27 . . PUNCT eurjchem-29 178 28     SPACE eurjchem-29 179 1 chem.1952 chem.1952 PROPN eurjchem-29 179 2 , , PUNCT eurjchem-29 179 3     SPACE eurjchem-29 179 4 59 59 NUM eurjchem-29 179 5 , , PUNCT eurjchem-29 179 6     SPACE eurjchem-29 179 7 198‐205 198‐205 NUM eurjchem-29 179 8 . . PUNCT eurjchem-29 179 9     SPACE eurjchem-29 180 1 [ [ X eurjchem-29 180 2 22 22 NUM eurjchem-29 180 3 ] ] PUNCT eurjchem-29 180 4 . . PUNCT eurjchem-29 180 5     SPACE eurjchem-29 180 6 singh singh PROPN eurjchem-29 180 7 , , PUNCT eurjchem-29 180 8     SPACE eurjchem-29 180 9 a. a. NOUN eurjchem-29 180 10 ; ; PUNCT eurjchem-29 180 11     SPACE eurjchem-29 180 12 latita latita NOUN eurjchem-29 180 13 , , PUNCT eurjchem-29 180 14     SPACE eurjchem-29 180 15 r. r. PROPN eurjchem-29 180 16 ; ; PUNCT eurjchem-29 180 17     SPACE eurjchem-29 180 18 r. r. PROPN eurjchem-29 180 19     SPACE eurjchem-29 180 20 dhakareg dhakareg NOUN eurjchem-29 180 21 , , PUNCT eurjchem-29 180 22     SPACE eurjchem-29 180 23 r. r. PROPN eurjchem-29 180 24 ; ; PUNCT eurjchem-29 180 25     SPACE eurjchem-29 180 26 saxena saxena PROPN eurjchem-29 180 27 , , PUNCT eurjchem-29 180 28     SPACE eurjchem-29 180 29 g. g. PROPN eurjchem-29 180 30     SPACE eurjchem-29 180 31 c. c. PROPN eurjchem-29 180 32     SPACE eurjchem-29 180 33 j. j. PROPN eurjchem-29 180 34     SPACE eurjchem-29 180 35 indian indian PROPN eurjchem-29 180 36     SPACE eurjchem-29 180 37 chem chem NOUN eurjchem-29 180 38 . . PUNCT eurjchem-29 180 39     SPACE eurjchem-29 180 40 soc soc PROPN eurjchem-29 180 41 . . PUNCT eurjchem-29 180 42     SPACE eurjchem-29 180 43 1996 1996 NUM eurjchem-29 180 44 , , PUNCT eurjchem-29 180 45     SPACE eurjchem-29 180 46 73 73 NUM eurjchem-29 180 47 , , PUNCT eurjchem-29 180 48     SPACE eurjchem-29 180 49 339‐348 339‐348 NUM eurjchem-29 180 50 . . PUNCT eurjchem-29 180 51     SPACE eurjchem-29 181 1 [ [ X eurjchem-29 181 2 23 23 NUM eurjchem-29 181 3 ] ] PUNCT eurjchem-29 181 4 . . PUNCT eurjchem-29 181 5     SPACE eurjchem-29 181 6 chaudhaxy chaudhaxy VERB eurjchem-29 181 7 , , PUNCT eurjchem-29 181 8     SPACE eurjchem-29 181 9 a. a. NOUN eurjchem-29 181 10 ; ; PUNCT eurjchem-29 181 11     SPACE eurjchem-29 181 12 singh singh NOUN eurjchem-29 181 13 , , PUNCT eurjchem-29 181 14     SPACE eurjchem-29 181 15 r. r. PROPN eurjchem-29 181 16     SPACE eurjchem-29 181 17 v. v. PROPN eurjchem-29 181 18     SPACE eurjchem-29 181 19 phosphorus phosphorus NOUN eurjchem-29 181 20 , , PUNCT eurjchem-29 181 21     SPACE eurjchem-29 181 22 sulfur sulfur NOUN eurjchem-29 181 23     SPACE eurjchem-29 181 24 silicon silicon NOUN eurjchem-29 181 25     SPACE eurjchem-29 181 26 relat relat NOUN eurjchem-29 181 27 . . PUNCT eurjchem-29 181 28     SPACE eurjchem-29 181 29 elem elem NOUN eurjchem-29 181 30 . . PUNCT eurjchem-29 181 31       SPACE eurjchem-29 182 1 2003 2003 NUM eurjchem-29 182 2 , , PUNCT eurjchem-29 182 3     SPACE eurjchem-29 182 4 178 178 NUM eurjchem-29 182 5 , , PUNCT eurjchem-29 182 6     SPACE eurjchem-29 182 7 603‐609 603‐609 PROPN eurjchem-29 182 8 . . PUNCT eurjchem-29 182 9     SPACE eurjchem-29 183 1 [ [ X eurjchem-29 183 2 24 24 NUM eurjchem-29 183 3 ] ] PUNCT eurjchem-29 183 4 . . PUNCT eurjchem-29 183 5     SPACE eurjchem-29 183 6 saraswati saraswati NOUN eurjchem-29 183 7 , , PUNCT eurjchem-29 183 8     SPACE eurjchem-29 183 9 s. s. PROPN eurjchem-29 183 10 ; ; PUNCT eurjchem-29 183 11     SPACE eurjchem-29 183 12 utpal utpal NOUN eurjchem-29 183 13 , , PUNCT eurjchem-29 183 14     SPACE eurjchem-29 183 15 d. d. NOUN eurjchem-29 183 16 ; ; PUNCT eurjchem-29 183 17     SPACE eurjchem-29 183 18 parikh parikh NOUN eurjchem-29 183 19 , , PUNCT eurjchem-29 183 20     SPACE eurjchem-29 183 21 a. a. NOUN eurjchem-29 183 22     SPACE eurjchem-29 183 23 r. r. PROPN eurjchem-29 183 24         SPACE eurjchem-29 183 25 j. j. PROPN eurjchem-29 183 26     SPACE eurjchem-29 183 27 indian indian PROPN eurjchem-29 183 28     SPACE eurjchem-29 183 29 chem chem NOUN eurjchem-29 183 30 . . PUNCT eurjchem-29 183 31     SPACE eurjchem-29 183 32 soc soc PROPN eurjchem-29 183 33 . . PUNCT eurjchem-29 183 34 , , PUNCT eurjchem-29 183 35     SPACE eurjchem-29 183 36 1994 1994 NUM eurjchem-29 183 37 , , PUNCT eurjchem-29 183 38     SPACE eurjchem-29 183 39 71 71 NUM eurjchem-29 183 40 , , PUNCT eurjchem-29 183 41     SPACE eurjchem-29 183 42 159‐167 159‐167 NUM eurjchem-29 183 43 . . PUNCT eurjchem-29 183 44     SPACE