id	sid	tid	token	lemma	pos
eurjchem-336	1	1	untitled	untitle	VERB
eurjchem-336	1	2	european	european	PROPN
eurjchem-336	1	3	journal	journal	PROPN
eurjchem-336	1	4	of	of	ADP
eurjchem-336	1	5	chemistry	chemistry	NOUN
eurjchem-336	1	6	2	2	NUM
eurjchem-336	1	7	(	(	PUNCT
eurjchem-336	1	8	2	2	NUM
eurjchem-336	1	9	)	)	PUNCT
eurjchem-336	1	10	(	(	PUNCT
eurjchem-336	1	11	2011	2011	NUM
eurjchem-336	1	12	)	)	PUNCT
eurjchem-336	1	13	223‐228	223‐228	PROPN
eurjchem-336	1	14	european	european	PROPN
eurjchem-336	1	15	journal	journal	PROPN
eurjchem-336	1	16	of	of	ADP
eurjchem-336	1	17	chemistry	chemistry	NOUN
eurjchem-336	1	18	issn	issn	PROPN
eurjchem-336	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-336	1	20	(	(	PUNCT
eurjchem-336	1	21	print	print	NOUN
eurjchem-336	1	22	)	)	PUNCT
eurjchem-336	1	23	/	/	SYM
eurjchem-336	1	24	issn	issn	PROPN
eurjchem-336	1	25	2153‐2257	2153‐2257	NUM
eurjchem-336	1	26	(	(	PUNCT
eurjchem-336	1	27	online	online	ADJ
eurjchem-336	1	28	)	)	PUNCT
eurjchem-336	1	29			NOUN
eurjchem-336	1	30	2011	2011	NUM
eurjchem-336	1	31	eurjchem	eurjchem	PROPN
eurjchem-336	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-336	1	33	/	/	SYM
eurjchem-336	1	34	eurjchem.2.2.223‐228.336	eurjchem.2.2.223‐228.336	NOUN
eurjchem-336	1	35	european	european	ADJ
eurjchem-336	1	36	journal	journal	PROPN
eurjchem-336	1	37	of	of	ADP
eurjchem-336	1	38	chemistry	chemistry	PROPN
eurjchem-336	1	39	journal	journal	PROPN
eurjchem-336	1	40	homepage	homepage	NOUN
eurjchem-336	1	41	:	:	PUNCT
eurjchem-336	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-336	2	1	a	a	DET
eurjchem-336	2	2	novel	novel	ADJ
eurjchem-336	2	3	and	and	CCONJ
eurjchem-336	2	4	efficient	efficient	ADJ
eurjchem-336	2	5	approach	approach	NOUN
eurjchem-336	2	6	for	for	ADP
eurjchem-336	2	7	the	the	DET
eurjchem-336	2	8	synthesis	synthesis	NOUN
eurjchem-336	2	9	of	of	ADP
eurjchem-336	2	10	new	new	ADJ
eurjchem-336	2	11	halo	halo	NOUN
eurjchem-336	2	12	substituted	substitute	VERB
eurjchem-336	2	13	2‐arylpyrazolo[4,3‐c	2‐arylpyrazolo[4,3‐c	NUM
eurjchem-336	2	14	]	]	PUNCT
eurjchem-336	2	15	coumarin	coumarin	NOUN
eurjchem-336	2	16	derivatives	derivative	NOUN
eurjchem-336	2	17	pradeep	pradeep	PROPN
eurjchem-336	2	18	lokhande	lokhande	PROPN
eurjchem-336	2	19	*	*	PROPN
eurjchem-336	2	20	,	,	PUNCT
eurjchem-336	2	21	kamal	kamal	PROPN
eurjchem-336	2	22	hasanzadeh	hasanzadeh	PROPN
eurjchem-336	2	23	and	and	CCONJ
eurjchem-336	2	24	shankaraiah	shankaraiah	PROPN
eurjchem-336	2	25	guruvaiah	guruvaiah	PROPN
eurjchem-336	2	26	konda	konda	PROPN
eurjchem-336	2	27	department	department	PROPN
eurjchem-336	2	28	of	of	ADP
eurjchem-336	2	29	chemistry	chemistry	NOUN
eurjchem-336	2	30	,	,	PUNCT
eurjchem-336	2	31	organic	organic	ADJ
eurjchem-336	2	32	research	research	NOUN
eurjchem-336	2	33	chemistry	chemistry	NOUN
eurjchem-336	2	34	,	,	PUNCT
eurjchem-336	2	35	university	university	NOUN
eurjchem-336	2	36	of	of	ADP
eurjchem-336	2	37	pune	pune	NOUN
eurjchem-336	2	38	,	,	PUNCT
eurjchem-336	2	39	pune‐411007	pune‐411007	PROPN
eurjchem-336	2	40	,	,	PUNCT
eurjchem-336	2	41	india	india	PROPN
eurjchem-336	2	42	*	*	PUNCT
eurjchem-336	2	43	corresponding	correspond	VERB
eurjchem-336	2	44	author	author	NOUN
eurjchem-336	2	45	at	at	ADP
eurjchem-336	2	46	:	:	PUNCT
eurjchem-336	2	47	department	department	NOUN
eurjchem-336	2	48	of	of	ADP
eurjchem-336	2	49	chemistry	chemistry	NOUN
eurjchem-336	2	50	,	,	PUNCT
eurjchem-336	2	51	organic	organic	ADJ
eurjchem-336	2	52	research	research	NOUN
eurjchem-336	2	53	chemistry	chemistry	NOUN
eurjchem-336	2	54	,	,	PUNCT
eurjchem-336	2	55	university	university	NOUN
eurjchem-336	2	56	of	of	ADP
eurjchem-336	2	57	pune	pune	NOUN
eurjchem-336	2	58	,	,	PUNCT
eurjchem-336	2	59	pune‐411007	pune‐411007	PROPN
eurjchem-336	2	60	,	,	PUNCT
eurjchem-336	2	61	india	india	PROPN
eurjchem-336	2	62	.	.	PUNCT
eurjchem-336	3	1	tel	tel	PROPN
eurjchem-336	3	2	.	.	PUNCT
eurjchem-336	3	3	:	:	PUNCT
eurjchem-336	4	1	+91.9604736297	+91.9604736297	ADJ
eurjchem-336	4	2	;	;	PUNCT
eurjchem-336	4	3	fax	fax	NOUN
eurjchem-336	4	4	:	:	PUNCT
eurjchem-336	4	5	+91.2025691728	+91.2025691728	PROPN
eurjchem-336	4	6	.	.	PUNCT
eurjchem-336	4	7	e‐mail	e‐mail	PUNCT
eurjchem-336	5	1	address	address	NOUN
eurjchem-336	5	2	:	:	PUNCT
eurjchem-336	5	3	pdlokhande@chem.unipune.ac.in	pdlokhande@chem.unipune.ac.in	PROPN
eurjchem-336	5	4	(	(	PUNCT
eurjchem-336	5	5	p.	p.	NOUN
eurjchem-336	5	6	lokhande	lokhande	PROPN
eurjchem-336	5	7	)	)	PUNCT
eurjchem-336	5	8	.	.	PUNCT
eurjchem-336	6	1	article	article	NOUN
eurjchem-336	6	2	information	information	PROPN
eurjchem-336	6	3	abstract	abstract	ADV
eurjchem-336	6	4	received	receive	VERB
eurjchem-336	6	5	:	:	PUNCT
eurjchem-336	6	6	20	20	NUM
eurjchem-336	6	7	november	november	PROPN
eurjchem-336	6	8	2010	2010	NUM
eurjchem-336	6	9	received	receive	VERB
eurjchem-336	6	10	in	in	ADP
eurjchem-336	6	11	revised	revise	VERB
eurjchem-336	6	12	form	form	NOUN
eurjchem-336	6	13	:	:	PUNCT
eurjchem-336	6	14	08	08	NUM
eurjchem-336	6	15	february	february	PROPN
eurjchem-336	6	16	2011	2011	NUM
eurjchem-336	6	17	accepted	accept	VERB
eurjchem-336	6	18	:	:	PUNCT
eurjchem-336	6	19	17	17	NUM
eurjchem-336	6	20	february	february	PROPN
eurjchem-336	6	21	2011	2011	NUM
eurjchem-336	6	22	online	online	NOUN
eurjchem-336	6	23	:	:	PUNCT
eurjchem-336	6	24	30	30	NUM
eurjchem-336	6	25	june	june	PROPN
eurjchem-336	6	26	2011	2011	NUM
eurjchem-336	6	27	keywords	keyword	VERB
eurjchem-336	6	28	a	a	DET
eurjchem-336	6	29	convenient	convenient	ADJ
eurjchem-336	6	30	protocol	protocol	NOUN
eurjchem-336	6	31	for	for	ADP
eurjchem-336	6	32	the	the	DET
eurjchem-336	6	33	efficient	efficient	ADJ
eurjchem-336	6	34	synthesis	synthesis	NOUN
eurjchem-336	6	35	of	of	ADP
eurjchem-336	6	36	2‐arylpyrazolo[4,3‐c]coumarins	2‐arylpyrazolo[4,3‐c]coumarins	NUM
eurjchem-336	6	37	is	be	AUX
eurjchem-336	6	38	described	describe	VERB
eurjchem-336	6	39	.	.	PUNCT
eurjchem-336	7	1	the	the	DET
eurjchem-336	7	2	synthesis	synthesis	NOUN
eurjchem-336	7	3	route	route	NOUN
eurjchem-336	7	4	involves	involve	VERB
eurjchem-336	7	5	molecular	molecular	ADJ
eurjchem-336	7	6	iodine	iodine	NOUN
eurjchem-336	7	7	catalyzed	catalyze	VERB
eurjchem-336	7	8	oxidative	oxidative	ADJ
eurjchem-336	7	9	cyclization	cyclization	NOUN
eurjchem-336	7	10	of	of	ADP
eurjchem-336	7	11	1‐	1‐	NUM
eurjchem-336	7	12	phenyl‐3‐(2'‐hydroxyaryl)‐4‐formyl	phenyl‐3‐(2'‐hydroxyaryl)‐4‐formyl	ADJ
eurjchem-336	7	13	pyrazoles	pyrazole	NOUN
eurjchem-336	7	14	in	in	ADP
eurjchem-336	7	15	dimethylsulfoxide	dimethylsulfoxide	ADV
eurjchem-336	7	16	.	.	PUNCT
eurjchem-336	8	1	during	during	ADP
eurjchem-336	8	2	the	the	DET
eurjchem-336	8	3	lactonisation	lactonisation	NOUN
eurjchem-336	8	4	of	of	ADP
eurjchem-336	8	5	4‐formylpyrazoles	4‐formylpyrazole	NOUN
eurjchem-336	8	6	,	,	PUNCT
eurjchem-336	8	7	we	we	PRON
eurjchem-336	8	8	found	find	VERB
eurjchem-336	8	9	that	that	SCONJ
eurjchem-336	8	10	iodine	iodine	NOUN
eurjchem-336	8	11	was	be	AUX
eurjchem-336	8	12	incorporated	incorporate	VERB
eurjchem-336	8	13	into	into	ADP
eurjchem-336	8	14	the	the	DET
eurjchem-336	8	15	unsubstituted	unsubstituted	ADJ
eurjchem-336	8	16	o	o	PROPN
eurjchem-336	8	17	/	/	SYM
eurjchem-336	8	18	p	p	NOUN
eurjchem-336	8	19	position	position	NOUN
eurjchem-336	8	20	of	of	ADP
eurjchem-336	8	21	the	the	DET
eurjchem-336	8	22	3‐(2'‐hydroxyaryl	3‐(2'‐hydroxyaryl	NOUN
eurjchem-336	8	23	)	)	PUNCT
eurjchem-336	8	24	group	group	NOUN
eurjchem-336	8	25	.	.	PUNCT
eurjchem-336	9	1	under	under	ADP
eurjchem-336	9	2	similar	similar	ADJ
eurjchem-336	9	3	conditions	condition	NOUN
eurjchem-336	9	4	o‐allyloxy	o‐allyloxy	PUNCT
eurjchem-336	9	5	derivative	derivative	NOUN
eurjchem-336	9	6	of	of	ADP
eurjchem-336	9	7	pyrazoles	pyrazole	NOUN
eurjchem-336	9	8	gave	give	VERB
eurjchem-336	9	9	same	same	ADJ
eurjchem-336	9	10	corresponding	corresponding	ADJ
eurjchem-336	9	11	lactone	lactone	NOUN
eurjchem-336	9	12	derivatives	derivative	NOUN
eurjchem-336	9	13	by	by	ADP
eurjchem-336	9	14	deallylation	deallylation	NOUN
eurjchem-336	9	15	,	,	PUNCT
eurjchem-336	9	16	lactonisation	lactonisation	NOUN
eurjchem-336	9	17	,	,	PUNCT
eurjchem-336	9	18	and	and	CCONJ
eurjchem-336	9	19	iodination	iodination	NOUN
eurjchem-336	9	20	in	in	ADP
eurjchem-336	9	21	one	one	NUM
eurjchem-336	9	22	step	step	NOUN
eurjchem-336	9	23	.	.	PUNCT
eurjchem-336	10	1	iodine	iodine	NOUN
eurjchem-336	10	2	lactonisation	lactonisation	NOUN
eurjchem-336	10	3	deallylation	deallylation	NOUN
eurjchem-336	10	4	2‐arylpyrazolo[4,3‐c]coumarins	2‐arylpyrazolo[4,3‐c]coumarins	NUM
eurjchem-336	10	5	oxidation	oxidation	ADJ
eurjchem-336	10	6	iodination	iodination	NOUN
eurjchem-336	10	7	1	1	NUM
eurjchem-336	10	8	.	.	X
eurjchem-336	11	1	introduction	introduction	NOUN
eurjchem-336	11	2	the	the	DET
eurjchem-336	11	3	diverse	diverse	ADJ
eurjchem-336	11	4	biological	biological	ADJ
eurjchem-336	11	5	activities	activity	NOUN
eurjchem-336	11	6	of	of	ADP
eurjchem-336	11	7	natural	natural	ADJ
eurjchem-336	11	8	and	and	CCONJ
eurjchem-336	11	9	synthetic	synthetic	ADJ
eurjchem-336	11	10	coumarins	coumarin	NOUN
eurjchem-336	11	11	as	as	ADP
eurjchem-336	11	12	coagulants	coagulant	NOUN
eurjchem-336	11	13	[	[	X
eurjchem-336	11	14	1	1	NUM
eurjchem-336	11	15	]	]	PUNCT
eurjchem-336	11	16	and	and	CCONJ
eurjchem-336	11	17	antithrombotics	antithrombotic	NOUN
eurjchem-336	12	1	[	[	X
eurjchem-336	12	2	2	2	NUM
eurjchem-336	12	3	]	]	PUNCT
eurjchem-336	12	4	are	be	AUX
eurjchem-336	12	5	well	well	ADV
eurjchem-336	12	6	known	known	ADJ
eurjchem-336	12	7	.	.	PUNCT
eurjchem-336	13	1	some	some	PRON
eurjchem-336	13	2	of	of	ADP
eurjchem-336	13	3	the	the	DET
eurjchem-336	13	4	coumarins	coumarin	NOUN
eurjchem-336	13	5	are	be	AUX
eurjchem-336	13	6	reported	report	VERB
eurjchem-336	13	7	as	as	ADP
eurjchem-336	13	8	anti	anti	ADJ
eurjchem-336	13	9	hiv	hiv	PROPN
eurjchem-336	13	10	agents	agent	NOUN
eurjchem-336	13	11	[	[	X
eurjchem-336	13	12	3	3	X
eurjchem-336	13	13	]	]	PUNCT
eurjchem-336	13	14	and	and	CCONJ
eurjchem-336	13	15	antioxidants	antioxidant	NOUN
eurjchem-336	13	16	[	[	X
eurjchem-336	13	17	4	4	NUM
eurjchem-336	13	18	]	]	PUNCT
eurjchem-336	13	19	.	.	PUNCT
eurjchem-336	14	1	many	many	ADJ
eurjchem-336	14	2	coumarin	coumarin	NOUN
eurjchem-336	14	3	derivatives	derivative	NOUN
eurjchem-336	14	4	are	be	AUX
eurjchem-336	14	5	known	know	VERB
eurjchem-336	14	6	as	as	ADP
eurjchem-336	14	7	free	free	ADJ
eurjchem-336	14	8	radical	radical	ADJ
eurjchem-336	14	9	scavengers	scavenger	NOUN
eurjchem-336	14	10	[	[	X
eurjchem-336	14	11	5	5	NUM
eurjchem-336	14	12	]	]	PUNCT
eurjchem-336	14	13	.	.	PUNCT
eurjchem-336	15	1	recent	recent	ADJ
eurjchem-336	15	2	work	work	NOUN
eurjchem-336	15	3	demonstrated	demonstrate	VERB
eurjchem-336	15	4	that	that	SCONJ
eurjchem-336	15	5	novobiocin	novobiocin	PROPN
eurjchem-336	15	6	was	be	AUX
eurjchem-336	15	7	observed	observe	VERB
eurjchem-336	15	8	to	to	PART
eurjchem-336	15	9	be	be	AUX
eurjchem-336	15	10	a	a	DET
eurjchem-336	15	11	dna‐gyrase	dna‐gyrase	ADJ
eurjchem-336	15	12	inhibitor	inhibitor	NOUN
eurjchem-336	15	13	[	[	X
eurjchem-336	15	14	6	6	NUM
eurjchem-336	15	15	]	]	PUNCT
eurjchem-336	15	16	that	that	PRON
eurjchem-336	15	17	binds	bind	VERB
eurjchem-336	15	18	to	to	ADP
eurjchem-336	15	19	the	the	DET
eurjchem-336	15	20	c‐terminal	c‐terminal	ADJ
eurjchem-336	15	21	nucleotide	nucleotide	NOUN
eurjchem-336	15	22	binding	bind	VERB
eurjchem-336	15	23	region	region	NOUN
eurjchem-336	15	24	of	of	ADP
eurjchem-336	15	25	heat	heat	NOUN
eurjchem-336	15	26	shock	shock	NOUN
eurjchem-336	15	27	protein‐90	protein‐90	PROPN
eurjchem-336	16	1	[	[	X
eurjchem-336	16	2	7	7	NUM
eurjchem-336	16	3	]	]	PUNCT
eurjchem-336	16	4	.	.	PUNCT
eurjchem-336	17	1	they	they	PRON
eurjchem-336	17	2	have	have	AUX
eurjchem-336	17	3	also	also	ADV
eurjchem-336	17	4	found	find	VERB
eurjchem-336	17	5	to	to	ADP
eurjchem-336	17	6	posses	posse	NOUN
eurjchem-336	17	7	vasorelaxant	vasorelaxant	ADJ
eurjchem-336	17	8	[	[	X
eurjchem-336	17	9	8	8	NUM
eurjchem-336	17	10	]	]	PUNCT
eurjchem-336	17	11	,	,	PUNCT
eurjchem-336	17	12	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-336	18	1	[	[	X
eurjchem-336	18	2	9	9	NUM
eurjchem-336	18	3	]	]	PUNCT
eurjchem-336	18	4	and	and	CCONJ
eurjchem-336	18	5	antitumor	antitumor	PROPN
eurjchem-336	18	6	[	[	X
eurjchem-336	18	7	10	10	NUM
eurjchem-336	18	8	]	]	PUNCT
eurjchem-336	18	9	activity	activity	NOUN
eurjchem-336	18	10	.	.	PUNCT
eurjchem-336	19	1	the	the	DET
eurjchem-336	19	2	incorporation	incorporation	NOUN
eurjchem-336	19	3	of	of	ADP
eurjchem-336	19	4	a	a	DET
eurjchem-336	19	5	fused	fuse	VERB
eurjchem-336	19	6	heterocyclic	heterocyclic	ADJ
eurjchem-336	19	7	moiety	moiety	NOUN
eurjchem-336	19	8	in	in	ADP
eurjchem-336	19	9	parent	parent	NOUN
eurjchem-336	19	10	coumarin	coumarin	NOUN
eurjchem-336	19	11	alters	alter	VERB
eurjchem-336	19	12	its	its	PRON
eurjchem-336	19	13	properties	property	NOUN
eurjchem-336	19	14	and	and	CCONJ
eurjchem-336	19	15	converts	convert	VERB
eurjchem-336	19	16	it	it	PRON
eurjchem-336	19	17	into	into	ADP
eurjchem-336	19	18	important	important	ADJ
eurjchem-336	19	19	derivatives	derivative	NOUN
eurjchem-336	19	20	[	[	X
eurjchem-336	19	21	11,12	11,12	NUM
eurjchem-336	19	22	]	]	PUNCT
eurjchem-336	19	23	.	.	PUNCT
eurjchem-336	20	1	large	large	ADJ
eurjchem-336	20	2	numbers	number	NOUN
eurjchem-336	20	3	of	of	ADP
eurjchem-336	20	4	heterocyclic	heterocyclic	NOUN
eurjchem-336	20	5	fused	fuse	VERB
eurjchem-336	20	6	and	and	CCONJ
eurjchem-336	20	7	heterocyclic	heterocyclic	ADJ
eurjchem-336	20	8	substituted	substitute	VERB
eurjchem-336	20	9	coumarin	coumarin	NOUN
eurjchem-336	20	10	derivatives	derivative	NOUN
eurjchem-336	20	11	is	be	AUX
eurjchem-336	20	12	used	use	VERB
eurjchem-336	20	13	as	as	ADP
eurjchem-336	20	14	drugs	drug	NOUN
eurjchem-336	20	15	and	and	CCONJ
eurjchem-336	20	16	dyes	dye	NOUN
eurjchem-336	21	1	[	[	X
eurjchem-336	21	2	13,14	13,14	NUM
eurjchem-336	21	3	]	]	PUNCT
eurjchem-336	21	4	.	.	PUNCT
eurjchem-336	22	1	the	the	DET
eurjchem-336	22	2	literature	literature	NOUN
eurjchem-336	22	3	reports	report	VERB
eurjchem-336	22	4	a	a	DET
eurjchem-336	22	5	short	short	ADJ
eurjchem-336	22	6	number	number	NOUN
eurjchem-336	22	7	of	of	ADP
eurjchem-336	22	8	synthetic	synthetic	ADJ
eurjchem-336	22	9	routes	route	NOUN
eurjchem-336	22	10	for	for	ADP
eurjchem-336	22	11	2‐arylpyrazolo[4,3‐c]coumarins	2‐arylpyrazolo[4,3‐c]coumarins	NUM
eurjchem-336	22	12	(	(	PUNCT
eurjchem-336	22	13	2‐arlychromeno[4,3‐	2‐arlychromeno[4,3‐	PROPN
eurjchem-336	22	14	c]pyrazol‐4(2h)‐ones	c]pyrazol‐4(2h)‐one	NOUN
eurjchem-336	22	15	)	)	PUNCT
eurjchem-336	22	16	,	,	PUNCT
eurjchem-336	22	17	such	such	ADJ
eurjchem-336	22	18	as	as	ADP
eurjchem-336	22	19	cyclization	cyclization	NOUN
eurjchem-336	22	20	of	of	ADP
eurjchem-336	22	21	the	the	DET
eurjchem-336	22	22	3‐hydrazone‐	3‐hydrazone‐	NUM
eurjchem-336	22	23	4‐chloro	4‐chloro	NUM
eurjchem-336	22	24	or	or	CCONJ
eurjchem-336	22	25	4‐hydroxy	4‐hydroxy	NUM
eurjchem-336	22	26	coumarins	coumarin	NOUN
eurjchem-336	22	27	,	,	PUNCT
eurjchem-336	22	28	which	which	PRON
eurjchem-336	22	29	were	be	AUX
eurjchem-336	22	30	relatively	relatively	ADV
eurjchem-336	22	31	unstable	unstable	ADJ
eurjchem-336	22	32	and	and	CCONJ
eurjchem-336	22	33	give	give	VERB
eurjchem-336	22	34	a	a	DET
eurjchem-336	22	35	mixture	mixture	NOUN
eurjchem-336	22	36	of	of	ADP
eurjchem-336	22	37	isomeric	isomeric	ADJ
eurjchem-336	22	38	1‐aryl	1‐aryl	NUM
eurjchem-336	22	39	and	and	CCONJ
eurjchem-336	22	40	2‐	2‐	NUM
eurjchem-336	22	41	arylpyrazolo[4,3‐c]coumarins	arylpyrazolo[4,3‐c]coumarin	NOUN
eurjchem-336	22	42	[	[	X
eurjchem-336	22	43	15,16	15,16	NUM
eurjchem-336	22	44	]	]	PUNCT
eurjchem-336	22	45	.	.	PUNCT
eurjchem-336	23	1	these	these	DET
eurjchem-336	23	2	compounds	compound	NOUN
eurjchem-336	23	3	were	be	AUX
eurjchem-336	23	4	studied	study	VERB
eurjchem-336	23	5	for	for	ADP
eurjchem-336	23	6	binding	bind	VERB
eurjchem-336	23	7	studies	study	NOUN
eurjchem-336	23	8	interaction	interaction	NOUN
eurjchem-336	23	9	with	with	ADP
eurjchem-336	23	10	the	the	DET
eurjchem-336	23	11	central	central	ADJ
eurjchem-336	23	12	benzodiazepine	benzodiazepine	NOUN
eurjchem-336	23	13	receptor	receptor	NOUN
eurjchem-336	23	14	[	[	X
eurjchem-336	23	15	17	17	NUM
eurjchem-336	23	16	]	]	PUNCT
eurjchem-336	23	17	.	.	PUNCT
eurjchem-336	24	1	considering	consider	VERB
eurjchem-336	24	2	the	the	DET
eurjchem-336	24	3	activity	activity	NOUN
eurjchem-336	24	4	profile	profile	NOUN
eurjchem-336	24	5	of	of	ADP
eurjchem-336	24	6	the	the	DET
eurjchem-336	24	7	2‐arylpyrazolo[4,3‐	2‐arylpyrazolo[4,3‐	PROPN
eurjchem-336	24	8	c]coumarins	c]coumarins	PROPN
eurjchem-336	24	9	,	,	PUNCT
eurjchem-336	24	10	we	we	PRON
eurjchem-336	24	11	decided	decide	VERB
eurjchem-336	24	12	to	to	PART
eurjchem-336	24	13	synthesis	synthesis	VERB
eurjchem-336	24	14	a	a	DET
eurjchem-336	24	15	new	new	ADJ
eurjchem-336	24	16	series	series	NOUN
eurjchem-336	24	17	of	of	ADP
eurjchem-336	24	18	halo	halo	PROPN
eurjchem-336	24	19	substituted	substitute	VERB
eurjchem-336	24	20	2‐arylpyrazolo[4,3‐c]coumarin	2‐arylpyrazolo[4,3‐c]coumarin	NUM
eurjchem-336	24	21	derivatives	derivative	NOUN
eurjchem-336	24	22	.	.	PUNCT
eurjchem-336	25	1	in	in	ADP
eurjchem-336	25	2	this	this	DET
eurjchem-336	25	3	account	account	NOUN
eurjchem-336	25	4	,	,	PUNCT
eurjchem-336	25	5	we	we	PRON
eurjchem-336	25	6	describe	describe	VERB
eurjchem-336	25	7	a	a	DET
eurjchem-336	25	8	new	new	ADJ
eurjchem-336	25	9	synthetic	synthetic	ADJ
eurjchem-336	25	10	route	route	NOUN
eurjchem-336	25	11	for	for	ADP
eurjchem-336	25	12	the	the	DET
eurjchem-336	25	13	synthesis	synthesis	NOUN
eurjchem-336	25	14	of	of	ADP
eurjchem-336	25	15	the	the	DET
eurjchem-336	25	16	title	title	NOUN
eurjchem-336	25	17	compounds	compound	VERB
eurjchem-336	25	18	from	from	ADP
eurjchem-336	25	19	the	the	DET
eurjchem-336	25	20	corresponding	correspond	VERB
eurjchem-336	25	21	3‐(2‐	3‐(2‐	NUM
eurjchem-336	25	22	hydroxyaryl)‐1‐phenyl‐1h‐pyrazole‐4‐carbaldehydes	hydroxyaryl)‐1‐phenyl‐1h‐pyrazole‐4‐carbaldehyde	NOUN
eurjchem-336	25	23	(	(	PUNCT
eurjchem-336	25	24	3	3	NUM
eurjchem-336	25	25	)	)	PUNCT
eurjchem-336	25	26	and	and	CCONJ
eurjchem-336	25	27	3‐(2‐(allyloxyaryl)‐1‐phenyl‐1h‐pyrazole‐4‐carbaldehydes	3‐(2‐(allyloxyaryl)‐1‐phenyl‐1h‐pyrazole‐4‐carbaldehydes	NUM
eurjchem-336	25	28	(	(	PUNCT
eurjchem-336	25	29	4	4	NUM
eurjchem-336	25	30	)	)	PUNCT
eurjchem-336	25	31	by	by	ADP
eurjchem-336	25	32	using	use	VERB
eurjchem-336	25	33	iodine	iodine	NOUN
eurjchem-336	25	34	in	in	ADP
eurjchem-336	25	35	dimethylsulfoxide	dimethylsulfoxide	ADJ
eurjchem-336	25	36	.	.	PUNCT
eurjchem-336	26	1	the	the	DET
eurjchem-336	26	2	use	use	NOUN
eurjchem-336	26	3	of	of	ADP
eurjchem-336	26	4	iodine	iodine	NOUN
eurjchem-336	26	5	for	for	ADP
eurjchem-336	26	6	synthetic	synthetic	ADJ
eurjchem-336	26	7	purpose	purpose	NOUN
eurjchem-336	26	8	has	have	AUX
eurjchem-336	26	9	gained	gain	VERB
eurjchem-336	26	10	significant	significant	ADJ
eurjchem-336	26	11	importance	importance	NOUN
eurjchem-336	26	12	.	.	PUNCT
eurjchem-336	27	1	the	the	DET
eurjchem-336	27	2	negligible	negligible	ADJ
eurjchem-336	27	3	toxicity	toxicity	NOUN
eurjchem-336	27	4	associated	associate	VERB
eurjchem-336	27	5	with	with	ADP
eurjchem-336	27	6	iodine	iodine	NOUN
eurjchem-336	27	7	,	,	PUNCT
eurjchem-336	27	8	in	in	ADP
eurjchem-336	27	9	conjunction	conjunction	NOUN
eurjchem-336	27	10	with	with	ADP
eurjchem-336	27	11	ease	ease	NOUN
eurjchem-336	27	12	of	of	ADP
eurjchem-336	27	13	handling	handling	NOUN
eurjchem-336	27	14	,	,	PUNCT
eurjchem-336	27	15	readily	readily	ADV
eurjchem-336	27	16	availability	availability	NOUN
eurjchem-336	27	17	,	,	PUNCT
eurjchem-336	27	18	low	low	ADJ
eurjchem-336	27	19	cost	cost	NOUN
eurjchem-336	27	20	and	and	CCONJ
eurjchem-336	27	21	mild	mild	ADJ
eurjchem-336	27	22	reaction	reaction	NOUN
eurjchem-336	27	23	conditions	condition	NOUN
eurjchem-336	27	24	employed	employ	VERB
eurjchem-336	27	25	has	have	AUX
eurjchem-336	27	26	resulted	result	VERB
eurjchem-336	27	27	in	in	ADP
eurjchem-336	27	28	its	its	PRON
eurjchem-336	27	29	application	application	NOUN
eurjchem-336	27	30	in	in	ADP
eurjchem-336	27	31	an	an	DET
eurjchem-336	27	32	increasing	increase	VERB
eurjchem-336	27	33	number	number	NOUN
eurjchem-336	27	34	of	of	ADP
eurjchem-336	27	35	diverse	diverse	ADJ
eurjchem-336	27	36	transformations	transformation	NOUN
eurjchem-336	27	37	[	[	X
eurjchem-336	27	38	18‐28	18‐28	NUM
eurjchem-336	27	39	]	]	PUNCT
eurjchem-336	27	40	.	.	PUNCT
eurjchem-336	28	1	in	in	ADP
eurjchem-336	28	2	continuation	continuation	NOUN
eurjchem-336	28	3	of	of	ADP
eurjchem-336	28	4	our	our	PRON
eurjchem-336	28	5	research	research	NOUN
eurjchem-336	28	6	programme	programme	NOUN
eurjchem-336	28	7	using	use	VERB
eurjchem-336	28	8	i2	i2	PROPN
eurjchem-336	28	9	/	/	SYM
eurjchem-336	28	10	dmso	dmso	NOUN
eurjchem-336	28	11	as	as	ADP
eurjchem-336	28	12	an	an	DET
eurjchem-336	28	13	efficient	efficient	ADJ
eurjchem-336	28	14	catalytic	catalytic	ADJ
eurjchem-336	28	15	system	system	NOUN
eurjchem-336	28	16	for	for	ADP
eurjchem-336	28	17	oxidation	oxidation	NOUN
eurjchem-336	28	18	of	of	ADP
eurjchem-336	28	19	pyrazoline	pyrazoline	NOUN
eurjchem-336	28	20	to	to	PART
eurjchem-336	28	21	pyrazole	pyrazole	NOUN
eurjchem-336	28	22	[	[	X
eurjchem-336	28	23	29	29	NUM
eurjchem-336	28	24	]	]	PUNCT
eurjchem-336	28	25	,	,	PUNCT
eurjchem-336	28	26	deallylation	deallylation	NOUN
eurjchem-336	28	27	and	and	CCONJ
eurjchem-336	28	28	preparation	preparation	NOUN
eurjchem-336	28	29	of	of	ADP
eurjchem-336	28	30	flavones	flavone	NOUN
eurjchem-336	28	31	from	from	ADP
eurjchem-336	28	32	2'‐	2'‐	NUM
eurjchem-336	28	33	allyloxychalcones	allyloxychalcone	NOUN
eurjchem-336	28	34	[	[	X
eurjchem-336	28	35	30	30	NUM
eurjchem-336	28	36	]	]	PUNCT
eurjchem-336	28	37	and	and	CCONJ
eurjchem-336	28	38	oxidation	oxidation	NOUN
eurjchem-336	28	39	of	of	ADP
eurjchem-336	28	40	dihydroflavone	dihydroflavone	NOUN
eurjchem-336	28	41	[	[	X
eurjchem-336	28	42	31	31	NUM
eurjchem-336	28	43	]	]	X
eurjchem-336	28	44	,	,	PUNCT
eurjchem-336	28	45	here	here	ADV
eurjchem-336	28	46	,	,	PUNCT
eurjchem-336	28	47	we	we	PRON
eurjchem-336	28	48	wish	wish	VERB
eurjchem-336	28	49	to	to	PART
eurjchem-336	28	50	report	report	VERB
eurjchem-336	28	51	some	some	DET
eurjchem-336	28	52	new	new	ADJ
eurjchem-336	28	53	halo	halo	NOUN
eurjchem-336	28	54	substituted	substitute	VERB
eurjchem-336	28	55	2‐	2‐	NUM
eurjchem-336	28	56	arylpyrazolo[4,3‐c]coumarins	arylpyrazolo[4,3‐c]coumarin	NOUN
eurjchem-336	28	57	under	under	ADP
eurjchem-336	28	58	mild	mild	ADJ
eurjchem-336	28	59	condition	condition	NOUN
eurjchem-336	28	60	.	.	PUNCT
eurjchem-336	29	1	to	to	ADP
eurjchem-336	29	2	the	the	DET
eurjchem-336	29	3	best	good	ADJ
eurjchem-336	29	4	of	of	ADP
eurjchem-336	29	5	our	our	PRON
eurjchem-336	29	6	knowledge	knowledge	NOUN
eurjchem-336	29	7	,	,	PUNCT
eurjchem-336	29	8	there	there	PRON
eurjchem-336	29	9	are	be	VERB
eurjchem-336	29	10	no	no	DET
eurjchem-336	29	11	earlier	early	ADJ
eurjchem-336	29	12	reports	report	NOUN
eurjchem-336	29	13	for	for	ADP
eurjchem-336	29	14	i2	i2	PROPN
eurjchem-336	29	15	/	/	SYM
eurjchem-336	29	16	dmso	dmso	NOUN
eurjchem-336	29	17	as	as	ADP
eurjchem-336	29	18	an	an	DET
eurjchem-336	29	19	efficient	efficient	ADJ
eurjchem-336	29	20	catalytic	catalytic	ADJ
eurjchem-336	29	21	system	system	NOUN
eurjchem-336	29	22	for	for	ADP
eurjchem-336	29	23	the	the	DET
eurjchem-336	29	24	synthesis	synthesis	NOUN
eurjchem-336	29	25	of	of	ADP
eurjchem-336	29	26	2‐	2‐	NUM
eurjchem-336	29	27	arylpyrazolo[4,3‐c]coumarins	arylpyrazolo[4,3‐c]coumarin	NOUN
eurjchem-336	29	28	.	.	PUNCT
eurjchem-336	30	1	2	2	X
eurjchem-336	30	2	.	.	X
eurjchem-336	30	3	experimental	experimental	ADJ
eurjchem-336	30	4	2.1	2.1	NUM
eurjchem-336	30	5	.	.	PUNCT
eurjchem-336	31	1	instrumentation	instrumentation	NOUN
eurjchem-336	31	2	1h	1h	NUM
eurjchem-336	31	3	nmr	nmr	NOUN
eurjchem-336	31	4	(	(	PUNCT
eurjchem-336	31	5	300	300	NUM
eurjchem-336	31	6	mhz	mhz	NOUN
eurjchem-336	31	7	)	)	PUNCT
eurjchem-336	31	8	and	and	CCONJ
eurjchem-336	31	9	13c	13c	NOUN
eurjchem-336	31	10	nmr	nmr	NOUN
eurjchem-336	31	11	(	(	PUNCT
eurjchem-336	31	12	75	75	NUM
eurjchem-336	31	13	mhz	mhz	NOUN
eurjchem-336	31	14	)	)	PUNCT
eurjchem-336	31	15	spectra	spectra	NOUN
eurjchem-336	31	16	were	be	AUX
eurjchem-336	31	17	recorded	record	VERB
eurjchem-336	31	18	on	on	ADP
eurjchem-336	31	19	a	a	DET
eurjchem-336	31	20	varian	varian	PROPN
eurjchem-336	31	21	vxr	vxr	PROPN
eurjchem-336	31	22	300	300	NUM
eurjchem-336	31	23	instrument	instrument	NOUN
eurjchem-336	31	24	at	at	ADP
eurjchem-336	31	25	293	293	NUM
eurjchem-336	31	26	k	k	NOUN
eurjchem-336	31	27	in	in	ADP
eurjchem-336	31	28	dmso‐d6	dmso‐d6	PROPN
eurjchem-336	31	29	.	.	PUNCT
eurjchem-336	32	1	chemical	chemical	NOUN
eurjchem-336	32	2	shift	shift	NOUN
eurjchem-336	32	3	values	value	NOUN
eurjchem-336	32	4	were	be	AUX
eurjchem-336	32	5	recorded	record	VERB
eurjchem-336	32	6	in	in	ADP
eurjchem-336	32	7	δ	δ	PROPN
eurjchem-336	32	8	units	unit	NOUN
eurjchem-336	32	9	(	(	PUNCT
eurjchem-336	32	10	ppm	ppm	NOUN
eurjchem-336	32	11	)	)	PUNCT
eurjchem-336	32	12	relative	relative	ADJ
eurjchem-336	32	13	to	to	ADP
eurjchem-336	32	14	me4si	me4si	PROPN
eurjchem-336	32	15	as	as	ADP
eurjchem-336	32	16	internal	internal	ADJ
eurjchem-336	32	17	standard	standard	NOUN
eurjchem-336	32	18	.	.	PUNCT
eurjchem-336	33	1	melting	melting	NOUN
eurjchem-336	33	2	points	point	NOUN
eurjchem-336	33	3	were	be	AUX
eurjchem-336	33	4	determined	determine	VERB
eurjchem-336	33	5	by	by	ADP
eurjchem-336	33	6	using	use	VERB
eurjchem-336	33	7	a	a	DET
eurjchem-336	33	8	buchi	buchi	NOUN
eurjchem-336	33	9	melting	melting	NOUN
eurjchem-336	33	10	point	point	NOUN
eurjchem-336	33	11	apparatus	apparatus	NOUN
eurjchem-336	33	12	.	.	PUNCT
eurjchem-336	34	1	infrared	infrared	PROPN
eurjchem-336	34	2	spectra	spectra	PROPN
eurjchem-336	34	3	(	(	PUNCT
eurjchem-336	34	4	ir	ir	NOUN
eurjchem-336	34	5	)	)	PUNCT
eurjchem-336	34	6	were	be	AUX
eurjchem-336	34	7	recorded	record	VERB
eurjchem-336	34	8	using	use	VERB
eurjchem-336	34	9	kbr	kbr	PROPN
eurjchem-336	34	10	pellets	pellet	NOUN
eurjchem-336	34	11	on	on	ADP
eurjchem-336	34	12	a	a	DET
eurjchem-336	34	13	perkin‐elmer	perkin‐elmer	PROPN
eurjchem-336	34	14	240c	240c	PROPN
eurjchem-336	34	15	analyzer	analyzer	NOUN
eurjchem-336	34	16	.	.	PUNCT
eurjchem-336	35	1	mass	mass	PROPN
eurjchem-336	35	2	spectra	spectra	PROPN
eurjchem-336	35	3	were	be	AUX
eurjchem-336	35	4	recorded	record	VERB
eurjchem-336	35	5	in	in	ADP
eurjchem-336	35	6	an	an	DET
eurjchem-336	35	7	ae‐ims‐30	ae‐ims‐30	ADJ
eurjchem-336	35	8	spectrometer	spectrometer	NOUN
eurjchem-336	35	9	.	.	PUNCT
eurjchem-336	36	1	thin	thin	ADJ
eurjchem-336	36	2	layer	layer	NOUN
eurjchem-336	36	3	chromatography	chromatography	NOUN
eurjchem-336	36	4	(	(	PUNCT
eurjchem-336	36	5	tlc	tlc	NOUN
eurjchem-336	36	6	)	)	PUNCT
eurjchem-336	36	7	was	be	AUX
eurjchem-336	36	8	performed	perform	VERB
eurjchem-336	36	9	on	on	ADP
eurjchem-336	36	10	silica	silica	NOUN
eurjchem-336	36	11	gel	gel	NOUN
eurjchem-336	36	12	60	60	NUM
eurjchem-336	36	13	pf254	pf254	PROPN
eurjchem-336	36	14	plates	plate	NOUN
eurjchem-336	36	15	or	or	CCONJ
eurjchem-336	36	16	aluminium	aluminium	NOUN
eurjchem-336	36	17	oxide	oxide	NOUN
eurjchem-336	36	18	plates	plate	NOUN
eurjchem-336	36	19	from	from	ADP
eurjchem-336	36	20	merck	merck	PROPN
eurjchem-336	36	21	.	.	PUNCT
eurjchem-336	37	1	elemental	elemental	PROPN
eurjchem-336	37	2	analyses	analysis	NOUN
eurjchem-336	37	3	were	be	AUX
eurjchem-336	37	4	performed	perform	VERB
eurjchem-336	37	5	on	on	ADP
eurjchem-336	37	6	a	a	DET
eurjchem-336	37	7	thermo	thermo	NOUN
eurjchem-336	37	8	flash	flash	NOUN
eurjchem-336	37	9	ea	ea	PROPN
eurjchem-336	37	10	1112	1112	NUM
eurjchem-336	37	11	analyzer	analyzer	NOUN
eurjchem-336	37	12	.	.	PUNCT
eurjchem-336	38	1	2.2	2.2	NUM
eurjchem-336	38	2	.	.	PUNCT
eurjchem-336	39	1	synthesis	synthesis	NOUN
eurjchem-336	39	2	2.2.1	2.2.1	NUM
eurjchem-336	39	3	.	.	PUNCT
eurjchem-336	39	4	general	general	ADJ
eurjchem-336	39	5	procedure	procedure	NOUN
eurjchem-336	39	6	for	for	ADP
eurjchem-336	39	7	the	the	DET
eurjchem-336	39	8	preparation	preparation	NOUN
eurjchem-336	39	9	of	of	ADP
eurjchem-336	39	10	substituted	substitute	VERB
eurjchem-336	39	11	acetophenones	acetophenone	NOUN
eurjchem-336	39	12	(	(	PUNCT
eurjchem-336	39	13	1a‐g	1a‐g	NOUN
eurjchem-336	39	14	)	)	PUNCT
eurjchem-336	39	15	224	224	NUM
eurjchem-336	39	16	lokhande	lokhande	VERB
eurjchem-336	39	17	et	et	PROPN
eurjchem-336	39	18	al	al	PROPN
eurjchem-336	39	19	.	.	PUNCT
eurjchem-336	39	20	/	/	SYM
eurjchem-336	39	21	european	european	PROPN
eurjchem-336	39	22	journal	journal	PROPN
eurjchem-336	39	23	of	of	ADP
eurjchem-336	39	24	chemistry	chemistry	NOUN
eurjchem-336	39	25	2	2	NUM
eurjchem-336	39	26	(	(	PUNCT
eurjchem-336	39	27	2	2	NUM
eurjchem-336	39	28	)	)	PUNCT
eurjchem-336	39	29	(	(	PUNCT
eurjchem-336	39	30	2011	2011	NUM
eurjchem-336	39	31	)	)	PUNCT
eurjchem-336	40	1	223‐228	223‐228	NUM
eurjchem-336	40	2	parent	parent	NOUN
eurjchem-336	40	3	5‐chloro‐2‐hydroxyacetophenone	5‐chloro‐2‐hydroxyacetophenone	NOUN
eurjchem-336	40	4	,	,	PUNCT
eurjchem-336	40	5	5‐bromo‐2‐	5‐bromo‐2‐	NUM
eurjchem-336	40	6	hydroxyacetophenone	hydroxyacetophenone	NOUN
eurjchem-336	40	7	,	,	PUNCT
eurjchem-336	40	8	3‐chloro‐2‐hydroxyacetophenone	3‐chloro‐2‐hydroxyacetophenone	NUM
eurjchem-336	40	9	,	,	PUNCT
eurjchem-336	40	10	3,5‐	3,5‐	NUM
eurjchem-336	40	11	dichloro‐2‐hydroxyacetophenone	dichloro‐2‐hydroxyacetophenone	PROPN
eurjchem-336	40	12	,	,	PUNCT
eurjchem-336	40	13	and	and	CCONJ
eurjchem-336	40	14	5‐methyl‐2‐hydroxy‐	5‐methyl‐2‐hydroxy‐	NUM
eurjchem-336	40	15	acetophenone	acetophenone	NOUN
eurjchem-336	40	16	were	be	AUX
eurjchem-336	40	17	synthesized	synthesize	VERB
eurjchem-336	40	18	from	from	ADP
eurjchem-336	40	19	p‐chloro	p‐chloro	PRON
eurjchem-336	40	20	,	,	PUNCT
eurjchem-336	40	21	p‐bromo	p‐bromo	NUM
eurjchem-336	40	22	,	,	PUNCT
eurjchem-336	40	23	o‐	o‐	ADJ
eurjchem-336	40	24	chloro	chloro	NOUN
eurjchem-336	40	25	,	,	PUNCT
eurjchem-336	40	26	2,4‐dichloro	2,4‐dichloro	NUM
eurjchem-336	40	27	and	and	CCONJ
eurjchem-336	40	28	p‐cresol	p‐cresol	VERB
eurjchem-336	40	29	phenols	phenol	NOUN
eurjchem-336	40	30	respectively	respectively	ADV
eurjchem-336	40	31	,	,	PUNCT
eurjchem-336	40	32	by	by	ADP
eurjchem-336	40	33	fries‐	fries‐	PROPN
eurjchem-336	40	34	rearrangement	rearrangement	NOUN
eurjchem-336	40	35	using	use	VERB
eurjchem-336	40	36	acetyl	acetyl	NOUN
eurjchem-336	40	37	chloride	chloride	NOUN
eurjchem-336	40	38	and	and	CCONJ
eurjchem-336	40	39	alcl3	alcl3	PUNCT
eurjchem-336	41	1	[	[	X
eurjchem-336	41	2	32	32	NUM
eurjchem-336	41	3	]	]	PUNCT
eurjchem-336	41	4	.	.	PUNCT
eurjchem-336	42	1	3,5‐	3,5‐	NUM
eurjchem-336	42	2	dibromo‐2‐hydroxyacetophenone	dibromo‐2‐hydroxyacetophenone	NOUN
eurjchem-336	42	3	and	and	CCONJ
eurjchem-336	42	4	3‐bromo‐5‐methyl‐2‐	3‐bromo‐5‐methyl‐2‐	NUM
eurjchem-336	42	5	hydroxyacetophenone	hydroxyacetophenone	NOUN
eurjchem-336	42	6	were	be	AUX
eurjchem-336	42	7	also	also	ADV
eurjchem-336	42	8	synthesized	synthesize	VERB
eurjchem-336	42	9	by	by	ADP
eurjchem-336	42	10	the	the	DET
eurjchem-336	42	11	bromination	bromination	NOUN
eurjchem-336	42	12	(	(	PUNCT
eurjchem-336	42	13	bromine	bromine	NOUN
eurjchem-336	42	14	in	in	ADP
eurjchem-336	42	15	acetic	acetic	ADJ
eurjchem-336	42	16	acid	acid	NOUN
eurjchem-336	42	17	)	)	PUNCT
eurjchem-336	42	18	method	method	NOUN
eurjchem-336	42	19	[	[	X
eurjchem-336	42	20	32	32	NUM
eurjchem-336	42	21	]	]	PUNCT
eurjchem-336	42	22	.	.	PUNCT
eurjchem-336	43	1	2.2.2	2.2.2	X
eurjchem-336	43	2	.	.	PUNCT
eurjchem-336	43	3	general	general	ADJ
eurjchem-336	43	4	procedure	procedure	NOUN
eurjchem-336	43	5	for	for	ADP
eurjchem-336	43	6	the	the	DET
eurjchem-336	43	7	preparation	preparation	NOUN
eurjchem-336	43	8	of	of	ADP
eurjchem-336	43	9	phenyl	phenyl	NOUN
eurjchem-336	43	10	hydrazones	hydrazone	NOUN
eurjchem-336	43	11	(	(	PUNCT
eurjchem-336	43	12	2a‐g	2a‐g	NOUN
eurjchem-336	43	13	)	)	PUNCT
eurjchem-336	43	14	to	to	ADP
eurjchem-336	43	15	a	a	DET
eurjchem-336	43	16	solution	solution	NOUN
eurjchem-336	43	17	of	of	ADP
eurjchem-336	43	18	the	the	DET
eurjchem-336	43	19	appropriate	appropriate	ADJ
eurjchem-336	43	20	2‐hydroxyacetophenone	2‐hydroxyacetophenone	NUM
eurjchem-336	43	21	derivatives	derivative	NOUN
eurjchem-336	43	22	(	(	PUNCT
eurjchem-336	43	23	24	24	NUM
eurjchem-336	43	24	mmol	mmol	NOUN
eurjchem-336	43	25	)	)	PUNCT
eurjchem-336	43	26	in	in	ADP
eurjchem-336	43	27	40	40	NUM
eurjchem-336	43	28	ml	ml	NOUN
eurjchem-336	43	29	methanol	methanol	NOUN
eurjchem-336	43	30	,	,	PUNCT
eurjchem-336	43	31	phenyl	phenyl	NOUN
eurjchem-336	43	32	hydrazine	hydrazine	NOUN
eurjchem-336	43	33	(	(	PUNCT
eurjchem-336	43	34	24	24	NUM
eurjchem-336	43	35	mmol	mmol	NOUN
eurjchem-336	43	36	)	)	PUNCT
eurjchem-336	43	37	was	be	AUX
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eurjchem-336	43	39	and	and	CCONJ
eurjchem-336	43	40	refluxed	refluxe	VERB
eurjchem-336	43	41	for	for	ADP
eurjchem-336	43	42	two	two	NUM
eurjchem-336	43	43	hours	hour	NOUN
eurjchem-336	43	44	.	.	PUNCT
eurjchem-336	44	1	after	after	ADP
eurjchem-336	44	2	cooling	cool	VERB
eurjchem-336	44	3	the	the	DET
eurjchem-336	44	4	reaction	reaction	NOUN
eurjchem-336	44	5	mixture	mixture	NOUN
eurjchem-336	44	6	the	the	DET
eurjchem-336	44	7	phenyl	phenyl	NOUN
eurjchem-336	44	8	hydrazone	hydrazone	NOUN
eurjchem-336	44	9	derivatives	derivative	NOUN
eurjchem-336	44	10	was	be	AUX
eurjchem-336	44	11	crystallized	crystallize	VERB
eurjchem-336	44	12	and	and	CCONJ
eurjchem-336	44	13	filtered	filter	VERB
eurjchem-336	44	14	,	,	PUNCT
eurjchem-336	44	15	the	the	DET
eurjchem-336	44	16	yield	yield	NOUN
eurjchem-336	44	17	was	be	AUX
eurjchem-336	44	18	91‐94	91‐94	NUM
eurjchem-336	44	19	%	%	NOUN
eurjchem-336	44	20	.	.	PUNCT
eurjchem-336	45	1	5‐chloro‐2‐hydroxy	5‐chloro‐2‐hydroxy	NUM
eurjchem-336	45	2	acetophenone	acetophenone	NOUN
eurjchem-336	45	3	phenylhydrazone	phenylhydrazone	NOUN
eurjchem-336	45	4	(	(	PUNCT
eurjchem-336	45	5	2a	2a	NUM
eurjchem-336	45	6	):	):	PUNCT
eurjchem-336	45	7	yield	yield	NOUN
eurjchem-336	45	8	:	:	PUNCT
eurjchem-336	45	9	91	91	NUM
eurjchem-336	45	10	%	%	NOUN
eurjchem-336	45	11	.	.	PUNCT
eurjchem-336	46	1	m.p	m.p	PROPN
eurjchem-336	46	2	.	.	PROPN
eurjchem-336	46	3	:	:	PUNCT
eurjchem-336	47	1	169‐171	169‐171	NUM
eurjchem-336	47	2	oc	oc	X
eurjchem-336	47	3	(	(	PUNCT
eurjchem-336	47	4	170	170	NUM
eurjchem-336	47	5	oc	oc	NOUN
eurjchem-336	47	6	[	[	X
eurjchem-336	47	7	33	33	NUM
eurjchem-336	47	8	]	]	NUM
eurjchem-336	47	9	)	)	PUNCT
eurjchem-336	47	10	.	.	PUNCT
eurjchem-336	48	1	ft‐ir	ft‐ir	NOUN
eurjchem-336	48	2	(	(	PUNCT
eurjchem-336	48	3	kbr	kbr	PROPN
eurjchem-336	48	4	,	,	PUNCT
eurjchem-336	48	5			PROPN
eurjchem-336	48	6	,	,	PUNCT
eurjchem-336	48	7	cm‐1	cm‐1	PROPN
eurjchem-336	48	8	):	):	PUNCT
eurjchem-336	48	9	3355	3355	NUM
eurjchem-336	48	10	,	,	PUNCT
eurjchem-336	48	11	1601	1601	NUM
eurjchem-336	48	12	.	.	PUNCT
eurjchem-336	49	1	1h	1h	NUM
eurjchem-336	49	2	nmr	nmr	NOUN
eurjchem-336	49	3	(	(	PUNCT
eurjchem-336	49	4	300	300	NUM
eurjchem-336	49	5	mhz	mhz	NOUN
eurjchem-336	49	6	,	,	PUNCT
eurjchem-336	49	7	cdcl3	cdcl3	NOUN
eurjchem-336	49	8	):	):	PUNCT
eurjchem-336	49	9	2.30	2.30	NUM
eurjchem-336	49	10	(	(	PUNCT
eurjchem-336	49	11	s	s	PROPN
eurjchem-336	49	12	,	,	PUNCT
eurjchem-336	49	13	3h	3h	NUM
eurjchem-336	49	14	)	)	PUNCT
eurjchem-336	49	15	,	,	PUNCT
eurjchem-336	49	16	6.93‐7.03	6.93‐7.03	NUM
eurjchem-336	49	17	(	(	PUNCT
eurjchem-336	49	18	m	m	PROPN
eurjchem-336	49	19	,	,	PUNCT
eurjchem-336	49	20	4h	4h	NOUN
eurjchem-336	49	21	)	)	PUNCT
eurjchem-336	49	22	,	,	PUNCT
eurjchem-336	49	23	7.16	7.16	NUM
eurjchem-336	49	24	(	(	PUNCT
eurjchem-336	49	25	dd	dd	PROPN
eurjchem-336	49	26	,	,	PUNCT
eurjchem-336	49	27	1h	1h	NUM
eurjchem-336	49	28	j1	j1	NOUN
eurjchem-336	49	29	=	=	PUNCT
eurjchem-336	49	30	8.4	8.4	NUM
eurjchem-336	49	31	hz	hz	NOUN
eurjchem-336	49	32	,	,	PUNCT
eurjchem-336	49	33	j2	j2	PROPN
eurjchem-336	49	34	=	=	PROPN
eurjchem-336	49	35	2.4	2.4	NUM
eurjchem-336	49	36	hz	hz	NOUN
eurjchem-336	49	37	)	)	PUNCT
eurjchem-336	49	38	,	,	PUNCT
eurjchem-336	49	39	7.29‐7.36	7.29‐7.36	NUM
eurjchem-336	49	40	(	(	PUNCT
eurjchem-336	49	41	m	m	PROPN
eurjchem-336	49	42	,	,	PUNCT
eurjchem-336	49	43	4h	4h	NOUN
eurjchem-336	49	44	)	)	PUNCT
eurjchem-336	49	45	,	,	PUNCT
eurjchem-336	49	46	12.49	12.49	NUM
eurjchem-336	49	47	(	(	PUNCT
eurjchem-336	49	48	s	s	PROPN
eurjchem-336	49	49	,	,	PUNCT
eurjchem-336	49	50	1h	1h	NUM
eurjchem-336	49	51	)	)	PUNCT
eurjchem-336	49	52	.	.	PUNCT
eurjchem-336	50	1	13c	13c	NOUN
eurjchem-336	50	2	nmr	nmr	NOUN
eurjchem-336	50	3	(	(	PUNCT
eurjchem-336	50	4	75	75	NUM
eurjchem-336	50	5	mhz	mhz	NOUN
eurjchem-336	50	6	,	,	PUNCT
eurjchem-336	50	7	cdcl3	cdcl3	NOUN
eurjchem-336	50	8	):	):	PUNCT
eurjchem-336	50	9	16.2	16.2	NUM
eurjchem-336	50	10	,	,	PUNCT
eurjchem-336	50	11	115.4	115.4	NUM
eurjchem-336	50	12	,	,	PUNCT
eurjchem-336	50	13	118.3	118.3	NUM
eurjchem-336	50	14	,	,	PUNCT
eurjchem-336	50	15	119.8	119.8	NUM
eurjchem-336	50	16	,	,	PUNCT
eurjchem-336	50	17	120.6	120.6	NUM
eurjchem-336	50	18	,	,	PUNCT
eurjchem-336	50	19	128.1	128.1	NUM
eurjchem-336	50	20	,	,	PUNCT
eurjchem-336	50	21	129.8	129.8	NUM
eurjchem-336	50	22	,	,	PUNCT
eurjchem-336	50	23	130.5	130.5	NUM
eurjchem-336	50	24	,	,	PUNCT
eurjchem-336	50	25	133.8	133.8	NUM
eurjchem-336	50	26	,	,	PUNCT
eurjchem-336	50	27	145.1	145.1	NUM
eurjchem-336	50	28	,	,	PUNCT
eurjchem-336	50	29	160.4	160.4	NUM
eurjchem-336	50	30	,	,	PUNCT
eurjchem-336	50	31	170.1	170.1	NUM
eurjchem-336	50	32	.	.	PUNCT
eurjchem-336	51	1	ms	ms	PROPN
eurjchem-336	51	2	(	(	PUNCT
eurjchem-336	51	3	ei	ei	PROPN
eurjchem-336	51	4	,	,	PUNCT
eurjchem-336	51	5	m	m	PROPN
eurjchem-336	51	6	/	/	SYM
eurjchem-336	51	7	z	z	X
eurjchem-336	51	8	):	):	PUNCT
eurjchem-336	51	9	262	262	NUM
eurjchem-336	51	10	(	(	PUNCT
eurjchem-336	51	11	m+2	m+2	NOUN
eurjchem-336	51	12	)	)	PUNCT
eurjchem-336	51	13	,	,	PUNCT
eurjchem-336	51	14	260	260	NUM
eurjchem-336	51	15	(	(	PUNCT
eurjchem-336	51	16	m+	m+	NOUN
eurjchem-336	51	17	)	)	PUNCT
eurjchem-336	51	18	,	,	PUNCT
eurjchem-336	51	19	243	243	NUM
eurjchem-336	51	20	.	.	PUNCT
eurjchem-336	52	1	anal	anal	PROPN
eurjchem-336	52	2	.	.	PUNCT
eurjchem-336	52	3	calcd	calcd	NOUN
eurjchem-336	52	4	.	.	PUNCT
eurjchem-336	53	1	for	for	ADP
eurjchem-336	53	2	c14h13n2ocl	c14h13n2ocl	VERB
eurjchem-336	53	3	:	:	PUNCT
eurjchem-336	53	4	c	c	X
eurjchem-336	53	5	,	,	PUNCT
eurjchem-336	53	6	64.61	64.61	NUM
eurjchem-336	53	7	;	;	PUNCT
eurjchem-336	53	8	h	h	NOUN
eurjchem-336	53	9	,	,	PUNCT
eurjchem-336	53	10	5.00	5.00	NUM
eurjchem-336	53	11	;	;	PUNCT
eurjchem-336	53	12	n	n	CCONJ
eurjchem-336	53	13	,	,	PUNCT
eurjchem-336	53	14	10.76	10.76	NUM
eurjchem-336	53	15	.	.	PUNCT
eurjchem-336	53	16	found	find	VERB
eurjchem-336	53	17	:	:	PUNCT
eurjchem-336	54	1	c	c	X
eurjchem-336	54	2	,	,	PUNCT
eurjchem-336	54	3	64.72	64.72	NUM
eurjchem-336	54	4	;	;	PUNCT
eurjchem-336	55	1	h	h	X
eurjchem-336	55	2	,	,	PUNCT
eurjchem-336	55	3	4.93	4.93	NUM
eurjchem-336	55	4	;	;	PUNCT
eurjchem-336	55	5	n	n	CCONJ
eurjchem-336	55	6	,	,	PUNCT
eurjchem-336	55	7	10.68	10.68	NUM
eurjchem-336	55	8	%	%	NOUN
eurjchem-336	55	9	.	.	PUNCT
eurjchem-336	56	1	5‐bromo‐2‐hydroxy	5‐bromo‐2‐hydroxy	NUM
eurjchem-336	56	2	acetophenone	acetophenone	NOUN
eurjchem-336	56	3	phenylhydrazone	phenylhydrazone	NOUN
eurjchem-336	56	4	(	(	PUNCT
eurjchem-336	56	5	2b	2b	NUM
eurjchem-336	56	6	):	):	PUNCT
eurjchem-336	56	7	yield	yield	NOUN
eurjchem-336	56	8	:	:	PUNCT
eurjchem-336	56	9	93	93	NUM
eurjchem-336	56	10	%	%	NOUN
eurjchem-336	56	11	.	.	PUNCT
eurjchem-336	57	1	m.p	m.p	PROPN
eurjchem-336	57	2	.	.	PROPN
eurjchem-336	57	3	:	:	PUNCT
eurjchem-336	58	1	163‐164	163‐164	NUM
eurjchem-336	58	2	oc	oc	NOUN
eurjchem-336	58	3	(	(	PUNCT
eurjchem-336	58	4	164	164	NUM
eurjchem-336	58	5	oc	oc	NOUN
eurjchem-336	58	6	[	[	X
eurjchem-336	58	7	33	33	NUM
eurjchem-336	58	8	]	]	NUM
eurjchem-336	58	9	)	)	PUNCT
eurjchem-336	58	10	.	.	PUNCT
eurjchem-336	59	1	ft‐ir	ft‐ir	NOUN
eurjchem-336	59	2	(	(	PUNCT
eurjchem-336	59	3	kbr	kbr	PROPN
eurjchem-336	59	4	,	,	PUNCT
eurjchem-336	59	5			PROPN
eurjchem-336	59	6	,	,	PUNCT
eurjchem-336	59	7	cm‐1	cm‐1	PROPN
eurjchem-336	59	8	):	):	PUNCT
eurjchem-336	59	9	3358	3358	NUM
eurjchem-336	59	10	,	,	PUNCT
eurjchem-336	59	11	1600	1600	NUM
eurjchem-336	59	12	.	.	PUNCT
eurjchem-336	60	1	1h	1h	NUM
eurjchem-336	60	2	nmr	nmr	NOUN
eurjchem-336	60	3	(	(	PUNCT
eurjchem-336	60	4	300	300	NUM
eurjchem-336	60	5	mhz	mhz	NOUN
eurjchem-336	60	6	,	,	PUNCT
eurjchem-336	60	7	cdcl3	cdcl3	NOUN
eurjchem-336	60	8	):	):	PUNCT
eurjchem-336	60	9	2.32	2.32	NUM
eurjchem-336	60	10	(	(	PUNCT
eurjchem-336	60	11	s	s	PROPN
eurjchem-336	60	12	,	,	PUNCT
eurjchem-336	60	13	3h	3h	NUM
eurjchem-336	60	14	)	)	PUNCT
eurjchem-336	60	15	,	,	PUNCT
eurjchem-336	60	16	7.01	7.01	NUM
eurjchem-336	60	17	(	(	PUNCT
eurjchem-336	60	18	d	d	PROPN
eurjchem-336	60	19	,	,	PUNCT
eurjchem-336	60	20	1h	1h	NUM
eurjchem-336	60	21	,	,	PUNCT
eurjchem-336	60	22	j	j	PROPN
eurjchem-336	60	23	=	=	SYM
eurjchem-336	60	24	7.5	7.5	NUM
eurjchem-336	60	25	hz	hz	NOUN
eurjchem-336	60	26	)	)	PUNCT
eurjchem-336	60	27	,	,	PUNCT
eurjchem-336	60	28	7.08‐7.12	7.08‐7.12	NUM
eurjchem-336	60	29	(	(	PUNCT
eurjchem-336	60	30	m	m	PROPN
eurjchem-336	60	31	,	,	PUNCT
eurjchem-336	60	32	3h	3h	NUM
eurjchem-336	60	33	)	)	PUNCT
eurjchem-336	60	34	,	,	PUNCT
eurjchem-336	60	35	7.21	7.21	NUM
eurjchem-336	60	36	(	(	PUNCT
eurjchem-336	60	37	dd	dd	PROPN
eurjchem-336	60	38	,	,	PUNCT
eurjchem-336	60	39	1h	1h	NUM
eurjchem-336	60	40	,	,	PUNCT
eurjchem-336	60	41	j1	j1	PROPN
eurjchem-336	60	42	=	=	NUM
eurjchem-336	60	43	7.8	7.8	NUM
eurjchem-336	60	44	hz	hz	NOUN
eurjchem-336	60	45	,	,	PUNCT
eurjchem-336	60	46	j2	j2	PROPN
eurjchem-336	60	47	=	=	SYM
eurjchem-336	60	48	2.7	2.7	NUM
eurjchem-336	60	49	hz	hz	NOUN
eurjchem-336	60	50	)	)	PUNCT
eurjchem-336	60	51	,	,	PUNCT
eurjchem-336	60	52	7.24‐7.34	7.24‐7.34	NUM
eurjchem-336	60	53	(	(	PUNCT
eurjchem-336	60	54	m	m	PROPN
eurjchem-336	60	55	,	,	PUNCT
eurjchem-336	60	56	3h	3h	NUM
eurjchem-336	60	57	)	)	PUNCT
eurjchem-336	60	58	,	,	PUNCT
eurjchem-336	60	59	7.44	7.44	NUM
eurjchem-336	60	60	(	(	PUNCT
eurjchem-336	60	61	d	d	PROPN
eurjchem-336	60	62	,	,	PUNCT
eurjchem-336	60	63	1h	1h	NUM
eurjchem-336	60	64	,	,	PUNCT
eurjchem-336	60	65	j	j	PROPN
eurjchem-336	60	66	=	=	SYM
eurjchem-336	60	67	2.7	2.7	NUM
eurjchem-336	60	68	hz	hz	NOUN
eurjchem-336	60	69	)	)	PUNCT
eurjchem-336	60	70	,	,	PUNCT
eurjchem-336	60	71	12.61	12.61	NUM
eurjchem-336	60	72	(	(	PUNCT
eurjchem-336	60	73	s	s	PROPN
eurjchem-336	60	74	,	,	PUNCT
eurjchem-336	60	75	1h	1h	NUM
eurjchem-336	60	76	)	)	PUNCT
eurjchem-336	60	77	.	.	PUNCT
eurjchem-336	61	1	13c	13c	NOUN
eurjchem-336	61	2	nmr	nmr	NOUN
eurjchem-336	61	3	(	(	PUNCT
eurjchem-336	61	4	75	75	NUM
eurjchem-336	61	5	mhz	mhz	NOUN
eurjchem-336	61	6	,	,	PUNCT
eurjchem-336	61	7	cdcl3	cdcl3	NOUN
eurjchem-336	61	8	):	):	PUNCT
eurjchem-336	61	9	15.8	15.8	NUM
eurjchem-336	61	10	,	,	PUNCT
eurjchem-336	61	11	114.9	114.9	NUM
eurjchem-336	61	12	,	,	PUNCT
eurjchem-336	61	13	117.1	117.1	NUM
eurjchem-336	61	14	,	,	PUNCT
eurjchem-336	61	15	119.4	119.4	NUM
eurjchem-336	61	16	,	,	PUNCT
eurjchem-336	61	17	119.8	119.8	NUM
eurjchem-336	61	18	,	,	PUNCT
eurjchem-336	61	19	121.5	121.5	NUM
eurjchem-336	61	20	,	,	PUNCT
eurjchem-336	61	21	128.2	128.2	NUM
eurjchem-336	61	22	,	,	PUNCT
eurjchem-336	61	23	136.3	136.3	NUM
eurjchem-336	61	24	,	,	PUNCT
eurjchem-336	61	25	137.1	137.1	NUM
eurjchem-336	61	26	,	,	PUNCT
eurjchem-336	61	27	145.4	145.4	NUM
eurjchem-336	61	28	,	,	PUNCT
eurjchem-336	61	29	159.2	159.2	NUM
eurjchem-336	61	30	,	,	PUNCT
eurjchem-336	61	31	168.2	168.2	NUM
eurjchem-336	61	32	.	.	PUNCT
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eurjchem-336	62	2	(	(	PUNCT
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eurjchem-336	62	8	):	):	PUNCT
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eurjchem-336	62	10	(	(	PUNCT
eurjchem-336	62	11	m+2	m+2	NOUN
eurjchem-336	62	12	)	)	PUNCT
eurjchem-336	62	13	,	,	PUNCT
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eurjchem-336	62	15	(	(	PUNCT
eurjchem-336	62	16	m+	m+	NUM
eurjchem-336	62	17	)	)	PUNCT
eurjchem-336	62	18	.	.	PUNCT
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eurjchem-336	63	2	.	.	PUNCT
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eurjchem-336	63	4	.	.	PUNCT
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eurjchem-336	64	3	:	:	PUNCT
eurjchem-336	64	4	c	c	NOUN
eurjchem-336	64	5	,	,	PUNCT
eurjchem-336	64	6	55.26	55.26	NUM
eurjchem-336	64	7	;	;	PUNCT
eurjchem-336	64	8	h	h	X
eurjchem-336	64	9	,	,	PUNCT
eurjchem-336	64	10	4.27	4.27	NUM
eurjchem-336	64	11	;	;	PUNCT
eurjchem-336	64	12	n	n	CCONJ
eurjchem-336	64	13	,	,	PUNCT
eurjchem-336	64	14	9.21	9.21	NUM
eurjchem-336	64	15	.	.	PUNCT
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eurjchem-336	64	17	:	:	PUNCT
eurjchem-336	65	1	c	c	X
eurjchem-336	65	2	,	,	PUNCT
eurjchem-336	65	3	55.31	55.31	NUM
eurjchem-336	65	4	;	;	PUNCT
eurjchem-336	65	5	h	h	NOUN
eurjchem-336	65	6	,	,	PUNCT
eurjchem-336	65	7	4.22	4.22	NUM
eurjchem-336	65	8	;	;	PUNCT
eurjchem-336	65	9	n	n	CCONJ
eurjchem-336	65	10	,	,	PUNCT
eurjchem-336	65	11	9.11	9.11	NUM
eurjchem-336	65	12	%	%	NOUN
eurjchem-336	65	13	.	.	PUNCT
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eurjchem-336	66	3	(	(	PUNCT
eurjchem-336	66	4	2c	2c	NUM
eurjchem-336	66	5	):	):	PUNCT
eurjchem-336	66	6	yield	yield	NOUN
eurjchem-336	66	7	:	:	PUNCT
eurjchem-336	66	8	92	92	NUM
eurjchem-336	66	9	%	%	NOUN
eurjchem-336	66	10	.	.	PUNCT
eurjchem-336	67	1	m.p	m.p	PROPN
eurjchem-336	67	2	.	.	PROPN
eurjchem-336	67	3	:	:	PUNCT
eurjchem-336	68	1	146‐148	146‐148	NUM
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eurjchem-336	68	3	.	.	PUNCT
eurjchem-336	68	4	ft‐ir	ft‐ir	NOUN
eurjchem-336	68	5	(	(	PUNCT
eurjchem-336	68	6	kbr	kbr	PROPN
eurjchem-336	68	7	,	,	PUNCT
eurjchem-336	68	8			PROPN
eurjchem-336	68	9	,	,	PUNCT
eurjchem-336	68	10	cm‐1	cm‐1	PROPN
eurjchem-336	68	11	):	):	PUNCT
eurjchem-336	68	12	3325	3325	NUM
eurjchem-336	68	13	,	,	PUNCT
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eurjchem-336	68	15	.	.	PUNCT
eurjchem-336	69	1	1h	1h	NUM
eurjchem-336	69	2	nmr	nmr	NOUN
eurjchem-336	69	3	(	(	PUNCT
eurjchem-336	69	4	300	300	NUM
eurjchem-336	69	5	mhz	mhz	NOUN
eurjchem-336	69	6	,	,	PUNCT
eurjchem-336	69	7	cdcl3	cdcl3	NOUN
eurjchem-336	69	8	):	):	PUNCT
eurjchem-336	69	9	2.34	2.34	NUM
eurjchem-336	69	10	(	(	PUNCT
eurjchem-336	69	11	s	s	PROPN
eurjchem-336	69	12	,	,	PUNCT
eurjchem-336	69	13	3h	3h	NUM
eurjchem-336	69	14	)	)	PUNCT
eurjchem-336	69	15	,	,	PUNCT
eurjchem-336	69	16	6.81	6.81	NUM
eurjchem-336	69	17	(	(	PUNCT
eurjchem-336	69	18	t	t	PROPN
eurjchem-336	69	19	,	,	PUNCT
eurjchem-336	69	20	1h	1h	NUM
eurjchem-336	69	21	,	,	PUNCT
eurjchem-336	69	22	j	j	PROPN
eurjchem-336	69	23	=	=	SYM
eurjchem-336	69	24	8.1	8.1	NUM
eurjchem-336	69	25	hz	hz	NOUN
eurjchem-336	69	26	)	)	PUNCT
eurjchem-336	69	27	,	,	PUNCT
eurjchem-336	69	28	6.94	6.94	NUM
eurjchem-336	69	29	(	(	PUNCT
eurjchem-336	69	30	t	t	PROPN
eurjchem-336	69	31	,	,	PUNCT
eurjchem-336	69	32	1h	1h	NUM
eurjchem-336	69	33	,	,	PUNCT
eurjchem-336	69	34	j	j	PROPN
eurjchem-336	69	35	=	=	SYM
eurjchem-336	69	36	7.2	7.2	NUM
eurjchem-336	69	37	hz	hz	NOUN
eurjchem-336	69	38	)	)	PUNCT
eurjchem-336	69	39	,	,	PUNCT
eurjchem-336	69	40	7.31	7.31	NUM
eurjchem-336	69	41	(	(	PUNCT
eurjchem-336	69	42	d	d	NOUN
eurjchem-336	69	43	,	,	PUNCT
eurjchem-336	69	44	2h	2h	NUM
eurjchem-336	69	45	,	,	PUNCT
eurjchem-336	69	46	j	j	PROPN
eurjchem-336	69	47	=	=	SYM
eurjchem-336	69	48	8.1	8.1	NUM
eurjchem-336	69	49	hz	hz	NOUN
eurjchem-336	69	50	)	)	PUNCT
eurjchem-336	69	51	,	,	PUNCT
eurjchem-336	69	52	7.27‐7.33	7.27‐7.33	NUM
eurjchem-336	69	53	(	(	PUNCT
eurjchem-336	69	54	m	m	PROPN
eurjchem-336	69	55	,	,	PUNCT
eurjchem-336	69	56	4h	4h	NOUN
eurjchem-336	69	57	)	)	PUNCT
eurjchem-336	69	58	,	,	PUNCT
eurjchem-336	69	59	12.63	12.63	NUM
eurjchem-336	69	60	(	(	PUNCT
eurjchem-336	69	61	s	s	PROPN
eurjchem-336	69	62	,	,	PUNCT
eurjchem-336	69	63	1h	1h	NUM
eurjchem-336	69	64	)	)	PUNCT
eurjchem-336	69	65	.	.	PUNCT
eurjchem-336	70	1	13c	13c	NOUN
eurjchem-336	70	2	nmr	nmr	NOUN
eurjchem-336	70	3	(	(	PUNCT
eurjchem-336	70	4	75	75	NUM
eurjchem-336	70	5	mhz	mhz	NOUN
eurjchem-336	70	6	,	,	PUNCT
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eurjchem-336	70	8	):	):	PUNCT
eurjchem-336	70	9	16.1	16.1	NUM
eurjchem-336	70	10	,	,	PUNCT
eurjchem-336	70	11	115.3	115.3	NUM
eurjchem-336	70	12	,	,	PUNCT
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eurjchem-336	70	14	,	,	PUNCT
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eurjchem-336	70	16	,	,	PUNCT
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eurjchem-336	70	18	,	,	PUNCT
eurjchem-336	70	19	125.6	125.6	NUM
eurjchem-336	70	20	,	,	PUNCT
eurjchem-336	70	21	129.7	129.7	NUM
eurjchem-336	70	22	,	,	PUNCT
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eurjchem-336	70	24	,	,	PUNCT
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eurjchem-336	70	26	,	,	PUNCT
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eurjchem-336	70	28	,	,	PUNCT
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eurjchem-336	70	30	,	,	PUNCT
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eurjchem-336	70	32	.	.	PUNCT
eurjchem-336	71	1	ms	ms	PROPN
eurjchem-336	71	2	(	(	PUNCT
eurjchem-336	71	3	ei	ei	PROPN
eurjchem-336	71	4	,	,	PUNCT
eurjchem-336	71	5	m	m	PROPN
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eurjchem-336	71	7	z	z	X
eurjchem-336	71	8	):	):	PUNCT
eurjchem-336	71	9	262	262	NUM
eurjchem-336	71	10	(	(	PUNCT
eurjchem-336	71	11	m+2	m+2	NOUN
eurjchem-336	71	12	)	)	PUNCT
eurjchem-336	71	13	,	,	PUNCT
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eurjchem-336	71	15	(	(	PUNCT
eurjchem-336	71	16	m+	m+	NUM
eurjchem-336	71	17	)	)	PUNCT
eurjchem-336	71	18	.	.	PUNCT
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eurjchem-336	72	2	.	.	PUNCT
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eurjchem-336	72	4	.	.	PUNCT
eurjchem-336	73	1	for	for	ADP
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eurjchem-336	73	3	:	:	PUNCT
eurjchem-336	73	4	c	c	X
eurjchem-336	73	5	,	,	PUNCT
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eurjchem-336	73	8	h	h	NOUN
eurjchem-336	73	9	,	,	PUNCT
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eurjchem-336	73	12	n	n	CCONJ
eurjchem-336	73	13	,	,	PUNCT
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eurjchem-336	73	17	:	:	PUNCT
eurjchem-336	74	1	c	c	X
eurjchem-336	74	2	,	,	PUNCT
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eurjchem-336	74	5	h	h	X
eurjchem-336	74	6	,	,	PUNCT
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eurjchem-336	74	8	;	;	PUNCT
eurjchem-336	74	9	n	n	CCONJ
eurjchem-336	74	10	,	,	PUNCT
eurjchem-336	74	11	10.81	10.81	NUM
eurjchem-336	74	12	%	%	NOUN
eurjchem-336	74	13	.	.	PUNCT
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eurjchem-336	75	4	(	(	PUNCT
eurjchem-336	75	5	2d	2d	NOUN
eurjchem-336	75	6	):	):	PUNCT
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eurjchem-336	75	8	:	:	PUNCT
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eurjchem-336	75	10	%	%	NOUN
eurjchem-336	75	11	.	.	PUNCT
eurjchem-336	76	1	m.p	m.p	PROPN
eurjchem-336	76	2	.	.	PROPN
eurjchem-336	76	3	:	:	PUNCT
eurjchem-336	77	1	132‐134	132‐134	NUM
eurjchem-336	77	2	oc	oc	X
eurjchem-336	77	3	(	(	PUNCT
eurjchem-336	77	4	133	133	NUM
eurjchem-336	77	5	oc	oc	NOUN
eurjchem-336	77	6	[	[	X
eurjchem-336	77	7	15	15	NUM
eurjchem-336	77	8	]	]	NUM
eurjchem-336	77	9	)	)	PUNCT
eurjchem-336	77	10	.	.	PUNCT
eurjchem-336	78	1	ft‐ir	ft‐ir	NOUN
eurjchem-336	78	2	(	(	PUNCT
eurjchem-336	78	3	kbr	kbr	PROPN
eurjchem-336	78	4	,	,	PUNCT
eurjchem-336	78	5			PROPN
eurjchem-336	78	6	,	,	PUNCT
eurjchem-336	78	7	cm‐1	cm‐1	PROPN
eurjchem-336	78	8	):	):	PUNCT
eurjchem-336	78	9	3344	3344	NUM
eurjchem-336	78	10	,	,	PUNCT
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eurjchem-336	78	12	.	.	PUNCT
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eurjchem-336	79	3	(	(	PUNCT
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eurjchem-336	79	6	,	,	PUNCT
eurjchem-336	79	7	cdcl3	cdcl3	NOUN
eurjchem-336	79	8	):	):	PUNCT
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eurjchem-336	79	11	s	s	PROPN
eurjchem-336	79	12	,	,	PUNCT
eurjchem-336	79	13	3h	3h	NUM
eurjchem-336	79	14	)	)	PUNCT
eurjchem-336	79	15	,	,	PUNCT
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eurjchem-336	79	17	(	(	PUNCT
eurjchem-336	79	18	t	t	PROPN
eurjchem-336	79	19	,	,	PUNCT
eurjchem-336	79	20	1h	1h	NUM
eurjchem-336	79	21	,	,	PUNCT
eurjchem-336	79	22	j	j	PROPN
eurjchem-336	79	23	=	=	SYM
eurjchem-336	79	24	7.5	7.5	NUM
eurjchem-336	79	25	hz	hz	NOUN
eurjchem-336	79	26	)	)	PUNCT
eurjchem-336	79	27	,	,	PUNCT
eurjchem-336	79	28	7.02	7.02	NUM
eurjchem-336	79	29	(	(	PUNCT
eurjchem-336	79	30	d	d	PROPN
eurjchem-336	79	31	,	,	PUNCT
eurjchem-336	79	32	2h	2h	NUM
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eurjchem-336	79	35	=	=	SYM
eurjchem-336	79	36	7.5	7.5	NUM
eurjchem-336	79	37	hz	hz	NOUN
eurjchem-336	79	38	)	)	PUNCT
eurjchem-336	79	39	,	,	PUNCT
eurjchem-336	79	40	7.28‐7.33	7.28‐7.33	NUM
eurjchem-336	79	41	(	(	PUNCT
eurjchem-336	79	42	m	m	PROPN
eurjchem-336	79	43	,	,	PUNCT
eurjchem-336	79	44	4h	4h	NOUN
eurjchem-336	79	45	)	)	PUNCT
eurjchem-336	79	46	,	,	PUNCT
eurjchem-336	79	47	7.39	7.39	NUM
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eurjchem-336	79	49	d	d	PROPN
eurjchem-336	79	50	,	,	PUNCT
eurjchem-336	79	51	1h	1h	NUM
eurjchem-336	79	52	,	,	PUNCT
eurjchem-336	79	53	j	j	PROPN
eurjchem-336	79	54	=	=	SYM
eurjchem-336	79	55	2.1	2.1	NUM
eurjchem-336	79	56	hz	hz	NOUN
eurjchem-336	79	57	)	)	PUNCT
eurjchem-336	79	58	,	,	PUNCT
eurjchem-336	79	59	13.18	13.18	NUM
eurjchem-336	79	60	(	(	PUNCT
eurjchem-336	79	61	s	s	PROPN
eurjchem-336	79	62	,	,	PUNCT
eurjchem-336	79	63	1h	1h	NUM
eurjchem-336	79	64	)	)	PUNCT
eurjchem-336	79	65	.	.	PUNCT
eurjchem-336	80	1	13c	13c	NOUN
eurjchem-336	80	2	nmr	nmr	NOUN
eurjchem-336	80	3	(	(	PUNCT
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eurjchem-336	80	6	,	,	PUNCT
eurjchem-336	80	7	cdcl3	cdcl3	NOUN
eurjchem-336	80	8	):	):	PUNCT
eurjchem-336	80	9	15.9	15.9	NUM
eurjchem-336	80	10	,	,	PUNCT
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eurjchem-336	80	12	,	,	PUNCT
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eurjchem-336	80	14	,	,	PUNCT
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eurjchem-336	80	16	,	,	PUNCT
eurjchem-336	80	17	126.7	126.7	NUM
eurjchem-336	80	18	,	,	PUNCT
eurjchem-336	80	19	129.3	129.3	NUM
eurjchem-336	80	20	,	,	PUNCT
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eurjchem-336	80	22	,	,	PUNCT
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eurjchem-336	80	24	,	,	PUNCT
eurjchem-336	80	25	135.6	135.6	NUM
eurjchem-336	80	26	,	,	PUNCT
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eurjchem-336	80	28	,	,	PUNCT
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eurjchem-336	80	30	,	,	PUNCT
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eurjchem-336	80	32	.	.	PUNCT
eurjchem-336	81	1	ms	ms	PROPN
eurjchem-336	81	2	(	(	PUNCT
eurjchem-336	81	3	ei	ei	PROPN
eurjchem-336	81	4	,	,	PUNCT
eurjchem-336	81	5	m	m	PROPN
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eurjchem-336	81	7	z	z	NOUN
eurjchem-336	81	8	):	):	PUNCT
eurjchem-336	81	9	296	296	NUM
eurjchem-336	81	10	(	(	PUNCT
eurjchem-336	81	11	m+2	m+2	NOUN
eurjchem-336	81	12	)	)	PUNCT
eurjchem-336	81	13	,	,	PUNCT
eurjchem-336	81	14	294(m+	294(m+	PROPN
eurjchem-336	81	15	)	)	PUNCT
eurjchem-336	81	16	.	.	PUNCT
eurjchem-336	82	1	anal	anal	PROPN
eurjchem-336	82	2	.	.	PUNCT
eurjchem-336	82	3	calcd	calcd	NOUN
eurjchem-336	82	4	.	.	PUNCT
eurjchem-336	83	1	for	for	SCONJ
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eurjchem-336	83	3	:	:	PUNCT
eurjchem-336	83	4	c	c	X
eurjchem-336	83	5	,	,	PUNCT
eurjchem-336	83	6	57.14	57.14	NUM
eurjchem-336	83	7	;	;	PUNCT
eurjchem-336	83	8	h	h	NOUN
eurjchem-336	83	9	,	,	PUNCT
eurjchem-336	83	10	4.08	4.08	NUM
eurjchem-336	83	11	;	;	PUNCT
eurjchem-336	83	12	n	n	CCONJ
eurjchem-336	83	13	,	,	PUNCT
eurjchem-336	83	14	9.52	9.52	NUM
eurjchem-336	83	15	.	.	PUNCT
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eurjchem-336	83	17	:	:	PUNCT
eurjchem-336	84	1	c	c	X
eurjchem-336	84	2	,	,	PUNCT
eurjchem-336	84	3	57.27	57.27	NUM
eurjchem-336	84	4	;	;	PUNCT
eurjchem-336	84	5	h	h	NOUN
eurjchem-336	84	6	,	,	PUNCT
eurjchem-336	84	7	4.11	4.11	NUM
eurjchem-336	84	8	;	;	PUNCT
eurjchem-336	84	9	n	n	CCONJ
eurjchem-336	84	10	,	,	PUNCT
eurjchem-336	84	11	9.61	9.61	NUM
eurjchem-336	84	12	%	%	NOUN
eurjchem-336	84	13	.	.	PUNCT
eurjchem-336	85	1	3,5‐dibromo‐2‐hydroxy	3,5‐dibromo‐2‐hydroxy	NUM
eurjchem-336	85	2	acetophenone	acetophenone	NOUN
eurjchem-336	85	3	phenylhydrazone	phenylhydrazone	NOUN
eurjchem-336	85	4	(	(	PUNCT
eurjchem-336	85	5	2e	2e	NOUN
eurjchem-336	85	6	):	):	PUNCT
eurjchem-336	85	7	yield	yield	NOUN
eurjchem-336	85	8	:	:	PUNCT
eurjchem-336	85	9	93	93	NUM
eurjchem-336	85	10	%	%	NOUN
eurjchem-336	85	11	.	.	PUNCT
eurjchem-336	86	1	m.p	m.p	PROPN
eurjchem-336	86	2	.	.	PROPN
eurjchem-336	86	3	:	:	PUNCT
eurjchem-336	87	1	151‐152	151‐152	NUM
eurjchem-336	87	2	oc	oc	NOUN
eurjchem-336	87	3	.	.	PUNCT
eurjchem-336	87	4	ft‐ir	ft‐ir	NOUN
eurjchem-336	87	5	(	(	PUNCT
eurjchem-336	87	6	kbr	kbr	PROPN
eurjchem-336	87	7	,	,	PUNCT
eurjchem-336	87	8			PROPN
eurjchem-336	87	9	,	,	PUNCT
eurjchem-336	87	10	cm‐1	cm‐1	PROPN
eurjchem-336	87	11	):	):	PUNCT
eurjchem-336	87	12	3358	3358	NUM
eurjchem-336	87	13	,	,	PUNCT
eurjchem-336	87	14	1608	1608	NUM
eurjchem-336	87	15	.	.	PUNCT
eurjchem-336	88	1	1h	1h	NUM
eurjchem-336	88	2	nmr	nmr	NOUN
eurjchem-336	88	3	(	(	PUNCT
eurjchem-336	88	4	300	300	NUM
eurjchem-336	88	5	mhz	mhz	NOUN
eurjchem-336	88	6	,	,	PUNCT
eurjchem-336	88	7	cdcl3	cdcl3	NOUN
eurjchem-336	88	8	):	):	PUNCT
eurjchem-336	88	9	2.34	2.34	NUM
eurjchem-336	88	10	(	(	PUNCT
eurjchem-336	88	11	s	s	PROPN
eurjchem-336	88	12	,	,	PUNCT
eurjchem-336	88	13	3h	3h	NUM
eurjchem-336	88	14	)	)	PUNCT
eurjchem-336	88	15	,	,	PUNCT
eurjchem-336	88	16	6.99	6.99	NUM
eurjchem-336	88	17	(	(	PUNCT
eurjchem-336	88	18	t	t	PROPN
eurjchem-336	88	19	,	,	PUNCT
eurjchem-336	88	20	1h	1h	NUM
eurjchem-336	88	21	,	,	PUNCT
eurjchem-336	88	22	j	j	PROPN
eurjchem-336	88	23	=	=	SYM
eurjchem-336	88	24	8.1	8.1	NUM
eurjchem-336	88	25	hz	hz	NOUN
eurjchem-336	88	26	)	)	PUNCT
eurjchem-336	88	27	,	,	PUNCT
eurjchem-336	88	28	7.09	7.09	NUM
eurjchem-336	88	29	(	(	PUNCT
eurjchem-336	88	30	d	d	PROPN
eurjchem-336	88	31	,	,	PUNCT
eurjchem-336	88	32	2h	2h	NUM
eurjchem-336	88	33	,	,	PUNCT
eurjchem-336	88	34	j	j	PROPN
eurjchem-336	88	35	=	=	SYM
eurjchem-336	88	36	7.1	7.1	NUM
eurjchem-336	88	37	hz	hz	NOUN
eurjchem-336	88	38	)	)	PUNCT
eurjchem-336	88	39	,	,	PUNCT
eurjchem-336	88	40	7.31	7.31	NUM
eurjchem-336	88	41	(	(	PUNCT
eurjchem-336	88	42	s	s	PROPN
eurjchem-336	88	43	,	,	PUNCT
eurjchem-336	88	44	1h	1h	NUM
eurjchem-336	88	45	)	)	PUNCT
eurjchem-336	88	46	,	,	PUNCT
eurjchem-336	88	47	7.32‐7.36	7.32‐7.36	NUM
eurjchem-336	88	48	(	(	PUNCT
eurjchem-336	88	49	m	m	PROPN
eurjchem-336	88	50	,	,	PUNCT
eurjchem-336	88	51	3h	3h	NUM
eurjchem-336	88	52	)	)	PUNCT
eurjchem-336	88	53	,	,	PUNCT
eurjchem-336	88	54	7.48	7.48	NUM
eurjchem-336	88	55	(	(	PUNCT
eurjchem-336	88	56	d	d	PROPN
eurjchem-336	88	57	,	,	PUNCT
eurjchem-336	88	58	1h	1h	NUM
eurjchem-336	88	59	,	,	PUNCT
eurjchem-336	88	60	j	j	PROPN
eurjchem-336	88	61	=	=	SYM
eurjchem-336	88	62	2.4	2.4	NUM
eurjchem-336	88	63	hz	hz	NOUN
eurjchem-336	88	64	)	)	PUNCT
eurjchem-336	88	65	,	,	PUNCT
eurjchem-336	88	66	12.87	12.87	NUM
eurjchem-336	88	67	(	(	PUNCT
eurjchem-336	88	68	s	s	PROPN
eurjchem-336	88	69	,	,	PUNCT
eurjchem-336	88	70	1h	1h	NUM
eurjchem-336	88	71	)	)	PUNCT
eurjchem-336	88	72	.	.	PUNCT
eurjchem-336	89	1	13c	13c	NOUN
eurjchem-336	89	2	nmr	nmr	NOUN
eurjchem-336	89	3	(	(	PUNCT
eurjchem-336	89	4	75	75	NUM
eurjchem-336	89	5	mhz	mhz	NOUN
eurjchem-336	89	6	,	,	PUNCT
eurjchem-336	89	7	cdcl3	cdcl3	NOUN
eurjchem-336	89	8	):	):	PUNCT
eurjchem-336	89	9	16.1	16.1	NUM
eurjchem-336	89	10	,	,	PUNCT
eurjchem-336	89	11	115.9	115.9	NUM
eurjchem-336	89	12	,	,	PUNCT
eurjchem-336	89	13	116.0	116.0	NUM
eurjchem-336	89	14	,	,	PUNCT
eurjchem-336	89	15	119.1	119.1	NUM
eurjchem-336	89	16	,	,	PUNCT
eurjchem-336	89	17	119.4	119.4	NUM
eurjchem-336	89	18	,	,	PUNCT
eurjchem-336	89	19	124.2	124.2	NUM
eurjchem-336	89	20	,	,	PUNCT
eurjchem-336	89	21	128.1	128.1	NUM
eurjchem-336	89	22	,	,	PUNCT
eurjchem-336	89	23	134.2	134.2	NUM
eurjchem-336	89	24	,	,	PUNCT
eurjchem-336	89	25	139.3	139.3	NUM
eurjchem-336	89	26	,	,	PUNCT
eurjchem-336	89	27	143.9	143.9	NUM
eurjchem-336	89	28	,	,	PUNCT
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eurjchem-336	89	30	,	,	PUNCT
eurjchem-336	89	31	169.2	169.2	NUM
eurjchem-336	89	32	.	.	PUNCT
eurjchem-336	90	1	ms	ms	NOUN
eurjchem-336	90	2	(	(	PUNCT
eurjchem-336	90	3	ei	ei	PROPN
eurjchem-336	90	4	,	,	PUNCT
eurjchem-336	90	5	m	m	PROPN
eurjchem-336	90	6	/	/	SYM
eurjchem-336	90	7	z	z	NOUN
eurjchem-336	90	8	):	):	PUNCT
eurjchem-336	90	9	386	386	NUM
eurjchem-336	90	10	(	(	PUNCT
eurjchem-336	90	11	m+4	m+4	PROPN
eurjchem-336	90	12	)	)	PUNCT
eurjchem-336	90	13	,	,	PUNCT
eurjchem-336	90	14	384	384	NUM
eurjchem-336	90	15	(	(	PUNCT
eurjchem-336	90	16	m+2	m+2	NOUN
eurjchem-336	90	17	)	)	PUNCT
eurjchem-336	90	18	,	,	PUNCT
eurjchem-336	90	19	382(m+	382(m+	NUM
eurjchem-336	90	20	)	)	PUNCT
eurjchem-336	90	21	.	.	PUNCT
eurjchem-336	91	1	anal	anal	PROPN
eurjchem-336	91	2	.	.	PUNCT
eurjchem-336	91	3	calcd	calcd	NOUN
eurjchem-336	91	4	.	.	PUNCT
eurjchem-336	92	1	for	for	ADP
eurjchem-336	92	2	c14h12n2obr2	c14h12n2obr2	PROPN
eurjchem-336	92	3	:	:	PUNCT
eurjchem-336	92	4	c	c	NOUN
eurjchem-336	92	5	,	,	PUNCT
eurjchem-336	92	6	43.97	43.97	NUM
eurjchem-336	92	7	;	;	PUNCT
eurjchem-336	92	8	h	h	NOUN
eurjchem-336	92	9	,	,	PUNCT
eurjchem-336	92	10	3.14	3.14	NUM
eurjchem-336	92	11	;	;	PUNCT
eurjchem-336	92	12	n	n	CCONJ
eurjchem-336	92	13	,	,	PUNCT
eurjchem-336	92	14	7.32	7.32	NUM
eurjchem-336	92	15	.	.	PUNCT
eurjchem-336	92	16	found	find	VERB
eurjchem-336	92	17	:	:	PUNCT
eurjchem-336	93	1	c	c	X
eurjchem-336	93	2	,	,	PUNCT
eurjchem-336	93	3	44.08	44.08	NUM
eurjchem-336	93	4	;	;	PUNCT
eurjchem-336	93	5	h	h	NOUN
eurjchem-336	93	6	,	,	PUNCT
eurjchem-336	93	7	3.20	3.20	NUM
eurjchem-336	93	8	;	;	PUNCT
eurjchem-336	93	9	n	n	CCONJ
eurjchem-336	93	10	,	,	PUNCT
eurjchem-336	93	11	7.42	7.42	NUM
eurjchem-336	93	12	%	%	NOUN
eurjchem-336	93	13	.	.	PUNCT
eurjchem-336	94	1	3‐bromo‐5‐chloro‐2‐hydroxy	3‐bromo‐5‐chloro‐2‐hydroxy	NUM
eurjchem-336	94	2	acetophenone	acetophenone	NOUN
eurjchem-336	94	3	phenylhydrazone	phenylhydrazone	NOUN
eurjchem-336	94	4	(	(	PUNCT
eurjchem-336	94	5	2f	2f	NUM
eurjchem-336	94	6	):	):	PUNCT
eurjchem-336	94	7	yield	yield	NOUN
eurjchem-336	94	8	:	:	PUNCT
eurjchem-336	94	9	93	93	NUM
eurjchem-336	94	10	%	%	NOUN
eurjchem-336	94	11	.	.	PUNCT
eurjchem-336	95	1	m.p	m.p	PROPN
eurjchem-336	95	2	.	.	PROPN
eurjchem-336	95	3	:	:	PUNCT
eurjchem-336	96	1	144‐145	144‐145	NUM
eurjchem-336	96	2	oc	oc	NOUN
eurjchem-336	96	3	.	.	PUNCT
eurjchem-336	96	4	ft‐ir	ft‐ir	NOUN
eurjchem-336	96	5	(	(	PUNCT
eurjchem-336	96	6	kbr	kbr	PROPN
eurjchem-336	96	7	,	,	PUNCT
eurjchem-336	96	8			PROPN
eurjchem-336	96	9	,	,	PUNCT
eurjchem-336	96	10	cm‐1	cm‐1	PROPN
eurjchem-336	96	11	):	):	PUNCT
eurjchem-336	96	12	3346	3346	NUM
eurjchem-336	96	13	,	,	PUNCT
eurjchem-336	96	14	1599	1599	NUM
eurjchem-336	96	15	.	.	PUNCT
eurjchem-336	97	1	1h	1h	NUM
eurjchem-336	97	2	nmr	nmr	NOUN
eurjchem-336	97	3	(	(	PUNCT
eurjchem-336	97	4	300	300	NUM
eurjchem-336	97	5	mhz	mhz	NOUN
eurjchem-336	97	6	,	,	PUNCT
eurjchem-336	97	7	cdcl3	cdcl3	NOUN
eurjchem-336	97	8	):	):	PUNCT
eurjchem-336	97	9	2.32	2.32	NUM
eurjchem-336	97	10	(	(	PUNCT
eurjchem-336	97	11	s	s	PROPN
eurjchem-336	97	12	,	,	PUNCT
eurjchem-336	97	13	3h	3h	NUM
eurjchem-336	97	14	)	)	PUNCT
eurjchem-336	97	15	,	,	PUNCT
eurjchem-336	97	16	6.98	6.98	NUM
eurjchem-336	97	17	(	(	PUNCT
eurjchem-336	97	18	t	t	PROPN
eurjchem-336	97	19	,	,	PUNCT
eurjchem-336	97	20	1h	1h	NUM
eurjchem-336	97	21	,	,	PUNCT
eurjchem-336	97	22	j	j	PROPN
eurjchem-336	97	23	=	=	SYM
eurjchem-336	97	24	7.2	7.2	NUM
eurjchem-336	97	25	hz	hz	NOUN
eurjchem-336	97	26	)	)	PUNCT
eurjchem-336	97	27	,	,	PUNCT
eurjchem-336	97	28	7.04	7.04	NUM
eurjchem-336	97	29	(	(	PUNCT
eurjchem-336	97	30	d	d	PROPN
eurjchem-336	97	31	,	,	PUNCT
eurjchem-336	97	32	2h	2h	NUM
eurjchem-336	97	33	,	,	PUNCT
eurjchem-336	97	34	j	j	PROPN
eurjchem-336	97	35	=	=	SYM
eurjchem-336	97	36	7.2	7.2	NUM
eurjchem-336	97	37	hz	hz	NOUN
eurjchem-336	97	38	)	)	PUNCT
eurjchem-336	97	39	,	,	PUNCT
eurjchem-336	97	40	7.29	7.29	NUM
eurjchem-336	97	41	(	(	PUNCT
eurjchem-336	97	42	s	s	PROPN
eurjchem-336	97	43	,	,	PUNCT
eurjchem-336	97	44	1h	1h	NUM
eurjchem-336	97	45	)	)	PUNCT
eurjchem-336	97	46	,	,	PUNCT
eurjchem-336	97	47	7.32‐7.34	7.32‐7.34	NUM
eurjchem-336	97	48	(	(	PUNCT
eurjchem-336	97	49	m	m	PROPN
eurjchem-336	97	50	,	,	PUNCT
eurjchem-336	97	51	3h	3h	NUM
eurjchem-336	97	52	)	)	PUNCT
eurjchem-336	97	53	,	,	PUNCT
eurjchem-336	97	54	7.47	7.47	NUM
eurjchem-336	97	55	(	(	PUNCT
eurjchem-336	97	56	d	d	PROPN
eurjchem-336	97	57	,	,	PUNCT
eurjchem-336	97	58	1h	1h	NUM
eurjchem-336	97	59	,	,	PUNCT
eurjchem-336	97	60	j	j	PROPN
eurjchem-336	97	61	=	=	SYM
eurjchem-336	97	62	2.4	2.4	NUM
eurjchem-336	97	63	hz	hz	NOUN
eurjchem-336	97	64	)	)	PUNCT
eurjchem-336	97	65	,	,	PUNCT
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eurjchem-336	97	68	s	s	PROPN
eurjchem-336	97	69	,	,	PUNCT
eurjchem-336	97	70	1h	1h	NUM
eurjchem-336	97	71	)	)	PUNCT
eurjchem-336	97	72	.	.	PUNCT
eurjchem-336	98	1	13c	13c	NOUN
eurjchem-336	98	2	nmr	nmr	NOUN
eurjchem-336	98	3	(	(	PUNCT
eurjchem-336	98	4	75	75	NUM
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eurjchem-336	98	6	,	,	PUNCT
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eurjchem-336	98	8	):	):	PUNCT
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eurjchem-336	98	10	,	,	PUNCT
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eurjchem-336	98	12	,	,	PUNCT
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eurjchem-336	98	14	,	,	PUNCT
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eurjchem-336	98	16	,	,	PUNCT
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eurjchem-336	98	18	,	,	PUNCT
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eurjchem-336	98	20	,	,	PUNCT
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eurjchem-336	98	22	,	,	PUNCT
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eurjchem-336	98	24	,	,	PUNCT
eurjchem-336	98	25	133.5	133.5	NUM
eurjchem-336	98	26	,	,	PUNCT
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eurjchem-336	98	28	,	,	PUNCT
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eurjchem-336	98	30	,	,	PUNCT
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eurjchem-336	98	32	.	.	PUNCT
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eurjchem-336	99	2	(	(	PUNCT
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eurjchem-336	99	4	,	,	PUNCT
eurjchem-336	99	5	m	m	PROPN
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eurjchem-336	99	7	z	z	NOUN
eurjchem-336	99	8	):	):	PUNCT
eurjchem-336	99	9	342	342	NUM
eurjchem-336	99	10	(	(	PUNCT
eurjchem-336	99	11	m+4	m+4	PROPN
eurjchem-336	99	12	)	)	PUNCT
eurjchem-336	99	13	,	,	PUNCT
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eurjchem-336	99	15	(	(	PUNCT
eurjchem-336	99	16	m+2	m+2	NOUN
eurjchem-336	99	17	)	)	PUNCT
eurjchem-336	99	18	,	,	PUNCT
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eurjchem-336	99	20	(	(	PUNCT
eurjchem-336	99	21	m+	m+	NUM
eurjchem-336	99	22	)	)	PUNCT
eurjchem-336	99	23	.	.	PUNCT
eurjchem-336	100	1	anal	anal	PROPN
eurjchem-336	100	2	.	.	PUNCT
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eurjchem-336	100	4	.	.	PUNCT
eurjchem-336	101	1	for	for	ADP
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eurjchem-336	101	3	:	:	PUNCT
eurjchem-336	101	4	c	c	X
eurjchem-336	101	5	,	,	PUNCT
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eurjchem-336	101	7	;	;	PUNCT
eurjchem-336	101	8	h	h	NOUN
eurjchem-336	101	9	,	,	PUNCT
eurjchem-336	101	10	3.55	3.55	NUM
eurjchem-336	101	11	;	;	PUNCT
eurjchem-336	101	12	n	n	CCONJ
eurjchem-336	101	13	,	,	PUNCT
eurjchem-336	101	14	8.28	8.28	NUM
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eurjchem-336	101	17	:	:	PUNCT
eurjchem-336	102	1	c	c	X
eurjchem-336	102	2	,	,	PUNCT
eurjchem-336	102	3	49.75	49.75	NUM
eurjchem-336	102	4	;	;	PUNCT
eurjchem-336	102	5	h	h	NOUN
eurjchem-336	102	6	,	,	PUNCT
eurjchem-336	102	7	3.61	3.61	NUM
eurjchem-336	102	8	;	;	PUNCT
eurjchem-336	102	9	n	n	CCONJ
eurjchem-336	102	10	,	,	PUNCT
eurjchem-336	102	11	8.34	8.34	NUM
eurjchem-336	102	12	%	%	NOUN
eurjchem-336	102	13	.	.	PUNCT
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eurjchem-336	103	5	(	(	PUNCT
eurjchem-336	103	6	2	2	NUM
eurjchem-336	103	7	g	g	NOUN
eurjchem-336	103	8	):	):	PUNCT
eurjchem-336	103	9	yield	yield	NOUN
eurjchem-336	103	10	:	:	PUNCT
eurjchem-336	103	11	93	93	NUM
eurjchem-336	103	12	%	%	NOUN
eurjchem-336	103	13	.	.	PUNCT
eurjchem-336	104	1	m.p	m.p	PROPN
eurjchem-336	104	2	.	.	PROPN
eurjchem-336	104	3	:	:	PUNCT
eurjchem-336	105	1	171‐173	171‐173	NUM
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eurjchem-336	105	3	.	.	PUNCT
eurjchem-336	105	4	ft‐ir	ft‐ir	NOUN
eurjchem-336	105	5	(	(	PUNCT
eurjchem-336	105	6	kbr	kbr	PROPN
eurjchem-336	105	7	,	,	PUNCT
eurjchem-336	105	8			PROPN
eurjchem-336	105	9	,	,	PUNCT
eurjchem-336	105	10	cm‐	cm‐	NOUN
eurjchem-336	105	11	1	1	NUM
eurjchem-336	105	12	):	):	PUNCT
eurjchem-336	105	13	3344	3344	NUM
eurjchem-336	105	14	,	,	PUNCT
eurjchem-336	105	15	1597	1597	NUM
eurjchem-336	105	16	.	.	PUNCT
eurjchem-336	106	1	1h	1h	NUM
eurjchem-336	106	2	nmr	nmr	NOUN
eurjchem-336	106	3	(	(	PUNCT
eurjchem-336	106	4	300	300	NUM
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eurjchem-336	106	6	,	,	PUNCT
eurjchem-336	106	7	cdcl3	cdcl3	NOUN
eurjchem-336	106	8	):	):	PUNCT
eurjchem-336	106	9	2.29	2.29	NUM
eurjchem-336	106	10	(	(	PUNCT
eurjchem-336	106	11	s	s	PROPN
eurjchem-336	106	12	,	,	PUNCT
eurjchem-336	106	13	3h	3h	NUM
eurjchem-336	106	14	)	)	PUNCT
eurjchem-336	106	15	,	,	PUNCT
eurjchem-336	106	16	2.32	2.32	NUM
eurjchem-336	106	17	(	(	PUNCT
eurjchem-336	106	18	s	s	PROPN
eurjchem-336	106	19	,	,	PUNCT
eurjchem-336	106	20	3h	3h	NUM
eurjchem-336	106	21	)	)	PUNCT
eurjchem-336	106	22	,	,	PUNCT
eurjchem-336	106	23	6.95	6.95	NUM
eurjchem-336	106	24	(	(	PUNCT
eurjchem-336	106	25	t	t	PROPN
eurjchem-336	106	26	,	,	PUNCT
eurjchem-336	106	27	1h	1h	NUM
eurjchem-336	106	28	,	,	PUNCT
eurjchem-336	106	29	j	j	PROPN
eurjchem-336	106	30	=	=	SYM
eurjchem-336	106	31	7.5	7.5	NUM
eurjchem-336	106	32	hz	hz	NOUN
eurjchem-336	106	33	)	)	PUNCT
eurjchem-336	106	34	,	,	PUNCT
eurjchem-336	106	35	7.04	7.04	NUM
eurjchem-336	106	36	(	(	PUNCT
eurjchem-336	106	37	d	d	PROPN
eurjchem-336	106	38	,	,	PUNCT
eurjchem-336	106	39	2h	2h	NUM
eurjchem-336	106	40	,	,	PUNCT
eurjchem-336	106	41	8.4	8.4	NUM
eurjchem-336	106	42	hz	hz	NOUN
eurjchem-336	106	43	)	)	PUNCT
eurjchem-336	106	44	,	,	PUNCT
eurjchem-336	106	45	7.16	7.16	NUM
eurjchem-336	106	46	(	(	PUNCT
eurjchem-336	106	47	s	s	PROPN
eurjchem-336	106	48	,	,	PUNCT
eurjchem-336	106	49	1h	1h	NUM
eurjchem-336	106	50	)	)	PUNCT
eurjchem-336	106	51	,	,	PUNCT
eurjchem-336	106	52	7.26‐7.31	7.26‐7.31	NUM
eurjchem-336	106	53	(	(	PUNCT
eurjchem-336	106	54	m	m	PROPN
eurjchem-336	106	55	,	,	PUNCT
eurjchem-336	106	56	3h	3h	NUM
eurjchem-336	106	57	)	)	PUNCT
eurjchem-336	106	58	,	,	PUNCT
eurjchem-336	106	59	7.32	7.32	NUM
eurjchem-336	106	60	(	(	PUNCT
eurjchem-336	106	61	d	d	PROPN
eurjchem-336	106	62	,	,	PUNCT
eurjchem-336	106	63	1h	1h	NUM
eurjchem-336	106	64	,	,	PUNCT
eurjchem-336	106	65	j	j	PROPN
eurjchem-336	106	66	=	=	SYM
eurjchem-336	106	67	1.8	1.8	NUM
eurjchem-336	106	68	hz	hz	NOUN
eurjchem-336	106	69	)	)	PUNCT
eurjchem-336	106	70	,	,	PUNCT
eurjchem-336	106	71	13.17	13.17	NUM
eurjchem-336	106	72	(	(	PUNCT
eurjchem-336	106	73	s	s	PROPN
eurjchem-336	106	74	,	,	PUNCT
eurjchem-336	106	75	1h	1h	NUM
eurjchem-336	106	76	)	)	PUNCT
eurjchem-336	106	77	.	.	PUNCT
eurjchem-336	107	1	13c	13c	NOUN
eurjchem-336	107	2	nmr	nmr	NOUN
eurjchem-336	107	3	(	(	PUNCT
eurjchem-336	107	4	75	75	NUM
eurjchem-336	107	5	mhz	mhz	NOUN
eurjchem-336	107	6	,	,	PUNCT
eurjchem-336	107	7	cdcl3	cdcl3	NOUN
eurjchem-336	107	8	):	):	PUNCT
eurjchem-336	107	9	16.1	16.1	NUM
eurjchem-336	107	10	,	,	PUNCT
eurjchem-336	107	11	22.9	22.9	NUM
eurjchem-336	107	12	,	,	PUNCT
eurjchem-336	107	13	112.6	112.6	NUM
eurjchem-336	107	14	,	,	PUNCT
eurjchem-336	107	15	115.8	115.8	NUM
eurjchem-336	107	16	,	,	PUNCT
eurjchem-336	107	17	117.0	117.0	NUM
eurjchem-336	107	18	,	,	PUNCT
eurjchem-336	107	19	122.1	122.1	NUM
eurjchem-336	107	20	,	,	PUNCT
eurjchem-336	107	21	128.3	128.3	NUM
eurjchem-336	107	22	,	,	PUNCT
eurjchem-336	107	23	128.9	128.9	NUM
eurjchem-336	107	24	,	,	PUNCT
eurjchem-336	107	25	134.0	134.0	NUM
eurjchem-336	107	26	,	,	PUNCT
eurjchem-336	107	27	138.2	138.2	NUM
eurjchem-336	107	28	,	,	PUNCT
eurjchem-336	107	29	142.4	142.4	NUM
eurjchem-336	107	30	,	,	PUNCT
eurjchem-336	107	31	157.7	157.7	NUM
eurjchem-336	107	32	,	,	PUNCT
eurjchem-336	107	33	169.4	169.4	NUM
eurjchem-336	107	34	.	.	PUNCT
eurjchem-336	108	1	ms	ms	NOUN
eurjchem-336	108	2	(	(	PUNCT
eurjchem-336	108	3	ei	ei	PROPN
eurjchem-336	108	4	,	,	PUNCT
eurjchem-336	108	5	m	m	PROPN
eurjchem-336	108	6	/	/	SYM
eurjchem-336	108	7	z	z	NOUN
eurjchem-336	108	8	):	):	PUNCT
eurjchem-336	108	9	320	320	NUM
eurjchem-336	108	10	(	(	PUNCT
eurjchem-336	108	11	m+2	m+2	NOUN
eurjchem-336	108	12	)	)	PUNCT
eurjchem-336	108	13	,	,	PUNCT
eurjchem-336	108	14	318	318	NUM
eurjchem-336	108	15	(	(	PUNCT
eurjchem-336	108	16	m+	m+	NUM
eurjchem-336	108	17	)	)	PUNCT
eurjchem-336	108	18	.	.	PUNCT
eurjchem-336	109	1	anal	anal	PROPN
eurjchem-336	109	2	.	.	PUNCT
eurjchem-336	109	3	calcd	calcd	NOUN
eurjchem-336	109	4	.	.	PUNCT
eurjchem-336	110	1	for	for	SCONJ
eurjchem-336	110	2	c15h15n2obr	c15h15n2obr	NOUN
eurjchem-336	110	3	:	:	PUNCT
eurjchem-336	110	4	c	c	X
eurjchem-336	110	5	,	,	PUNCT
eurjchem-336	110	6	56.60	56.60	NUM
eurjchem-336	110	7	;	;	PUNCT
eurjchem-336	110	8	h	h	NOUN
eurjchem-336	110	9	,	,	PUNCT
eurjchem-336	110	10	4.71	4.71	NUM
eurjchem-336	110	11	;	;	PUNCT
eurjchem-336	110	12	n	n	CCONJ
eurjchem-336	110	13	,	,	PUNCT
eurjchem-336	110	14	8.80	8.80	NUM
eurjchem-336	110	15	.	.	PUNCT
eurjchem-336	110	16	found	find	VERB
eurjchem-336	110	17	:	:	PUNCT
eurjchem-336	111	1	c	c	X
eurjchem-336	111	2	,	,	PUNCT
eurjchem-336	111	3	56.71	56.71	NUM
eurjchem-336	111	4	;	;	PUNCT
eurjchem-336	111	5	h	h	NOUN
eurjchem-336	111	6	,	,	PUNCT
eurjchem-336	111	7	4.67	4.67	NUM
eurjchem-336	111	8	;	;	PUNCT
eurjchem-336	111	9	n	n	CCONJ
eurjchem-336	111	10	,	,	PUNCT
eurjchem-336	111	11	8.69	8.69	NUM
eurjchem-336	111	12	%	%	NOUN
eurjchem-336	111	13	.	.	PUNCT
eurjchem-336	112	1	2.2.3	2.2.3	X
eurjchem-336	112	2	.	.	PUNCT
eurjchem-336	112	3	general	general	ADJ
eurjchem-336	112	4	procedure	procedure	NOUN
eurjchem-336	112	5	for	for	ADP
eurjchem-336	112	6	the	the	DET
eurjchem-336	112	7	preparation	preparation	NOUN
eurjchem-336	112	8	of	of	ADP
eurjchem-336	112	9	3‐aryl‐1‐	3‐aryl‐1‐	NUM
eurjchem-336	112	10	phenyl‐1h‐pyrazole‐4‐carbaldehyde	phenyl‐1h‐pyrazole‐4‐carbaldehyde	PROPN
eurjchem-336	112	11	(	(	PUNCT
eurjchem-336	112	12	3a‐g	3a‐g	NOUN
eurjchem-336	112	13	)	)	PUNCT
eurjchem-336	112	14	the	the	DET
eurjchem-336	112	15	derivatives	derivative	NOUN
eurjchem-336	112	16	of	of	ADP
eurjchem-336	112	17	2‐hydroxyacetophenone	2‐hydroxyacetophenone	NUM
eurjchem-336	112	18	phenyl	phenyl	NOUN
eurjchem-336	112	19	hydrazone	hydrazone	NOUN
eurjchem-336	112	20	(	(	PUNCT
eurjchem-336	112	21	0.01	0.01	NUM
eurjchem-336	112	22	mol	mol	NOUN
eurjchem-336	112	23	)	)	PUNCT
eurjchem-336	112	24	was	be	AUX
eurjchem-336	112	25	dissolved	dissolve	VERB
eurjchem-336	112	26	in	in	ADP
eurjchem-336	112	27	dmf	dmf	PROPN
eurjchem-336	112	28	(	(	PUNCT
eurjchem-336	112	29	15	15	NUM
eurjchem-336	112	30	ml	ml	NOUN
eurjchem-336	112	31	)	)	PUNCT
eurjchem-336	112	32	and	and	CCONJ
eurjchem-336	112	33	then	then	ADV
eurjchem-336	112	34	pocl3	pocl3	PROPN
eurjchem-336	112	35	(	(	PUNCT
eurjchem-336	112	36	0.03	0.03	NUM
eurjchem-336	112	37	mol	mol	NOUN
eurjchem-336	112	38	)	)	PUNCT
eurjchem-336	112	39	was	be	AUX
eurjchem-336	112	40	added	add	VERB
eurjchem-336	112	41	drop	drop	NOUN
eurjchem-336	112	42	wise	wise	ADJ
eurjchem-336	112	43	at	at	ADP
eurjchem-336	112	44	0	0	NUM
eurjchem-336	112	45	oc	oc	NOUN
eurjchem-336	112	46	.	.	PUNCT
eurjchem-336	113	1	after	after	ADP
eurjchem-336	113	2	a	a	DET
eurjchem-336	113	3	complete	complete	ADJ
eurjchem-336	113	4	addition	addition	NOUN
eurjchem-336	113	5	of	of	ADP
eurjchem-336	113	6	pocl3	pocl3	NOUN
eurjchem-336	113	7	,	,	PUNCT
eurjchem-336	113	8	the	the	DET
eurjchem-336	113	9	reaction	reaction	NOUN
eurjchem-336	113	10	mixture	mixture	NOUN
eurjchem-336	113	11	warmed	warm	VERB
eurjchem-336	113	12	at	at	ADP
eurjchem-336	113	13	room	room	NOUN
eurjchem-336	113	14	temperature	temperature	NOUN
eurjchem-336	113	15	and	and	CCONJ
eurjchem-336	113	16	heated	heat	VERB
eurjchem-336	113	17	at	at	ADP
eurjchem-336	113	18	60‐70	60‐70	NUM
eurjchem-336	113	19	oc	oc	NOUN
eurjchem-336	113	20	for	for	ADP
eurjchem-336	113	21	2.5‐3	2.5‐3	PROPN
eurjchem-336	113	22	h.the	h.the	DET
eurjchem-336	113	23	reaction	reaction	NOUN
eurjchem-336	113	24	was	be	AUX
eurjchem-336	113	25	poured	pour	VERB
eurjchem-336	113	26	onto	onto	ADP
eurjchem-336	113	27	crushed	crushed	ADJ
eurjchem-336	113	28	ice	ice	NOUN
eurjchem-336	113	29	and	and	CCONJ
eurjchem-336	113	30	then	then	ADV
eurjchem-336	113	31	neutralized	neutralize	VERB
eurjchem-336	113	32	with	with	ADP
eurjchem-336	113	33	10	10	NUM
eurjchem-336	113	34	%	%	NOUN
eurjchem-336	113	35	aqueous	aqueous	ADJ
eurjchem-336	113	36	naoh	naoh	NOUN
eurjchem-336	113	37	solution	solution	NOUN
eurjchem-336	113	38	.	.	PUNCT
eurjchem-336	114	1	the	the	DET
eurjchem-336	114	2	precipitate	precipitate	NOUN
eurjchem-336	114	3	was	be	AUX
eurjchem-336	114	4	filtered	filter	VERB
eurjchem-336	114	5	,	,	PUNCT
eurjchem-336	114	6	strongly	strongly	ADV
eurjchem-336	114	7	washed	wash	VERB
eurjchem-336	114	8	with	with	ADP
eurjchem-336	114	9	water	water	NOUN
eurjchem-336	114	10	and	and	CCONJ
eurjchem-336	114	11	crystallized	crystallize	VERB
eurjchem-336	114	12	from	from	ADP
eurjchem-336	114	13	ethanol	ethanol	NOUN
eurjchem-336	114	14	.	.	PUNCT
eurjchem-336	115	1	3‐(5‐chloro‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	3‐(5‐chloro‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	NUM
eurjchem-336	115	2	carbaldehyde	carbaldehyde	NOUN
eurjchem-336	115	3	(	(	PUNCT
eurjchem-336	115	4	3a	3a	NUM
eurjchem-336	115	5	):	):	PUNCT
eurjchem-336	115	6	yield	yield	NOUN
eurjchem-336	115	7	:	:	PUNCT
eurjchem-336	115	8	84	84	NUM
eurjchem-336	115	9	%	%	NOUN
eurjchem-336	115	10	.	.	PUNCT
eurjchem-336	116	1	m.p	m.p	PROPN
eurjchem-336	116	2	.	.	PROPN
eurjchem-336	116	3	:	:	PUNCT
eurjchem-336	117	1	132‐134	132‐134	NUM
eurjchem-336	117	2	oc	oc	NOUN
eurjchem-336	117	3	.	.	PUNCT
eurjchem-336	117	4	ft‐ir	ft‐ir	NOUN
eurjchem-336	117	5	(	(	PUNCT
eurjchem-336	117	6	kbr	kbr	PROPN
eurjchem-336	117	7	,	,	PUNCT
eurjchem-336	117	8			PROPN
eurjchem-336	117	9	,	,	PUNCT
eurjchem-336	117	10	cm‐1	cm‐1	PROPN
eurjchem-336	117	11	):	):	PUNCT
eurjchem-336	117	12	3450	3450	NUM
eurjchem-336	117	13	,	,	PUNCT
eurjchem-336	117	14	1683	1683	NUM
eurjchem-336	117	15	,	,	PUNCT
eurjchem-336	117	16	1657	1657	NUM
eurjchem-336	117	17	.	.	PUNCT
eurjchem-336	118	1	1h	1h	NUM
eurjchem-336	118	2	nmr	nmr	NOUN
eurjchem-336	118	3	(	(	PUNCT
eurjchem-336	118	4	300	300	NUM
eurjchem-336	118	5	mhz	mhz	NOUN
eurjchem-336	118	6	,	,	PUNCT
eurjchem-336	118	7	cdcl3	cdcl3	NOUN
eurjchem-336	118	8	):	):	PUNCT
eurjchem-336	118	9	7.02	7.02	NUM
eurjchem-336	118	10	(	(	PUNCT
eurjchem-336	118	11	d	d	PROPN
eurjchem-336	118	12	,	,	PUNCT
eurjchem-336	118	13	1h	1h	NUM
eurjchem-336	118	14	,	,	PUNCT
eurjchem-336	118	15	j	j	PROPN
eurjchem-336	118	16	=	=	PROPN
eurjchem-336	118	17	8.4	8.4	NUM
eurjchem-336	118	18	hz	hz	NOUN
eurjchem-336	118	19	)	)	PUNCT
eurjchem-336	118	20	,	,	PUNCT
eurjchem-336	118	21	7.25	7.25	NUM
eurjchem-336	118	22	(	(	PUNCT
eurjchem-336	118	23	dd	dd	PROPN
eurjchem-336	118	24	,	,	PUNCT
eurjchem-336	118	25	1h	1h	NUM
eurjchem-336	118	26	,	,	PUNCT
eurjchem-336	118	27	j1	j1	PROPN
eurjchem-336	118	28	=	=	NUM
eurjchem-336	118	29	8.7	8.7	NUM
eurjchem-336	118	30	hz	hz	NOUN
eurjchem-336	118	31	,	,	PUNCT
eurjchem-336	118	32	j2	j2	PROPN
eurjchem-336	118	33	=	=	PROPN
eurjchem-336	118	34	2.4	2.4	NUM
eurjchem-336	118	35	hz	hz	NOUN
eurjchem-336	118	36	)	)	PUNCT
eurjchem-336	118	37	,	,	PUNCT
eurjchem-336	118	38	7.43	7.43	NUM
eurjchem-336	118	39	(	(	PUNCT
eurjchem-336	118	40	t	t	PROPN
eurjchem-336	118	41	,	,	PUNCT
eurjchem-336	118	42	1h	1h	NUM
eurjchem-336	118	43	,	,	PUNCT
eurjchem-336	118	44	j	j	PROPN
eurjchem-336	118	45	=	=	SYM
eurjchem-336	118	46	7.2	7.2	NUM
eurjchem-336	118	47	hz	hz	NOUN
eurjchem-336	118	48	)	)	PUNCT
eurjchem-336	118	49	,	,	PUNCT
eurjchem-336	118	50	7.54	7.54	NUM
eurjchem-336	118	51	(	(	PUNCT
eurjchem-336	118	52	t	t	PROPN
eurjchem-336	118	53	,	,	PUNCT
eurjchem-336	118	54	2h	2h	NUM
eurjchem-336	118	55	,	,	PUNCT
eurjchem-336	118	56	j	j	PROPN
eurjchem-336	118	57	=	=	SYM
eurjchem-336	118	58	7.8	7.8	NUM
eurjchem-336	118	59	hz	hz	NOUN
eurjchem-336	118	60	)	)	PUNCT
eurjchem-336	118	61	,	,	PUNCT
eurjchem-336	118	62	7.69	7.69	NUM
eurjchem-336	118	63	(	(	PUNCT
eurjchem-336	118	64	d	d	PROPN
eurjchem-336	118	65	,	,	PUNCT
eurjchem-336	118	66	2h	2h	NUM
eurjchem-336	118	67	,	,	PUNCT
eurjchem-336	118	68	j	j	PROPN
eurjchem-336	118	69	=	=	SYM
eurjchem-336	118	70	7.8	7.8	NUM
eurjchem-336	118	71	hz	hz	NOUN
eurjchem-336	118	72	)	)	PUNCT
eurjchem-336	118	73	,	,	PUNCT
eurjchem-336	118	74	8.07	8.07	NUM
eurjchem-336	118	75	(	(	PUNCT
eurjchem-336	118	76	d	d	PROPN
eurjchem-336	118	77	,	,	PUNCT
eurjchem-336	118	78	1h	1h	NUM
eurjchem-336	118	79	,	,	PUNCT
eurjchem-336	118	80	j	j	PROPN
eurjchem-336	118	81	=	=	SYM
eurjchem-336	118	82	2.1hz	2.1hz	PROPN
eurjchem-336	118	83	)	)	PUNCT
eurjchem-336	118	84	,	,	PUNCT
eurjchem-336	118	85	8.56	8.56	NUM
eurjchem-336	118	86	(	(	PUNCT
eurjchem-336	118	87	s	s	PROPN
eurjchem-336	118	88	,	,	PUNCT
eurjchem-336	118	89	1h	1h	NUM
eurjchem-336	118	90	)	)	PUNCT
eurjchem-336	118	91	,	,	PUNCT
eurjchem-336	118	92	10.14	10.14	NUM
eurjchem-336	118	93	(	(	PUNCT
eurjchem-336	118	94	s	s	PROPN
eurjchem-336	118	95	,	,	PUNCT
eurjchem-336	118	96	2h	2h	NUM
eurjchem-336	118	97	)	)	PUNCT
eurjchem-336	118	98	.	.	PUNCT
eurjchem-336	119	1	13c	13c	NOUN
eurjchem-336	119	2	nmr	nmr	NOUN
eurjchem-336	119	3	(	(	PUNCT
eurjchem-336	119	4	75	75	NUM
eurjchem-336	119	5	mhz	mhz	NOUN
eurjchem-336	119	6	,	,	PUNCT
eurjchem-336	119	7	cdcl3	cdcl3	NOUN
eurjchem-336	119	8	):	):	PUNCT
eurjchem-336	119	9	116.4	116.4	NUM
eurjchem-336	119	10	,	,	PUNCT
eurjchem-336	119	11	118.5	118.5	NUM
eurjchem-336	119	12	,	,	PUNCT
eurjchem-336	119	13	119.3	119.3	NUM
eurjchem-336	119	14	,	,	PUNCT
eurjchem-336	119	15	122.8	122.8	NUM
eurjchem-336	119	16	,	,	PUNCT
eurjchem-336	119	17	124.2	124.2	NUM
eurjchem-336	119	18	,	,	PUNCT
eurjchem-336	119	19	128.4	128.4	NUM
eurjchem-336	119	20	,	,	PUNCT
eurjchem-336	119	21	129.0	129.0	NUM
eurjchem-336	119	22	,	,	PUNCT
eurjchem-336	119	23	129.7	129.7	NUM
eurjchem-336	119	24	,	,	PUNCT
eurjchem-336	119	25	130.6	130.6	NUM
eurjchem-336	119	26	,	,	PUNCT
eurjchem-336	119	27	133.5	133.5	NUM
eurjchem-336	119	28	,	,	PUNCT
eurjchem-336	119	29	137.6	137.6	NUM
eurjchem-336	119	30	,	,	PUNCT
eurjchem-336	119	31	150.9	150.9	NUM
eurjchem-336	119	32	,	,	PUNCT
eurjchem-336	119	33	154.4	154.4	NUM
eurjchem-336	119	34	,	,	PUNCT
eurjchem-336	119	35	183.2	183.2	NUM
eurjchem-336	119	36	.	.	PUNCT
eurjchem-336	120	1	ms	ms	NOUN
eurjchem-336	120	2	(	(	PUNCT
eurjchem-336	120	3	ei	ei	PROPN
eurjchem-336	120	4	,	,	PUNCT
eurjchem-336	120	5	m	m	PROPN
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eurjchem-336	120	7	z	z	PROPN
eurjchem-336	120	8	):	):	PUNCT
eurjchem-336	120	9	298	298	NUM
eurjchem-336	120	10	(	(	PUNCT
eurjchem-336	120	11	m+	m+	NUM
eurjchem-336	120	12	)	)	PUNCT
eurjchem-336	120	13	.	.	PUNCT
eurjchem-336	121	1	anal	anal	PROPN
eurjchem-336	121	2	.	.	PUNCT
eurjchem-336	121	3	calcd	calcd	NOUN
eurjchem-336	121	4	.	.	PUNCT
eurjchem-336	122	1	for	for	SCONJ
eurjchem-336	122	2	c16h11n2o2cl	c16h11n2o2cl	PROPN
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eurjchem-336	122	4	c	c	X
eurjchem-336	122	5	,	,	PUNCT
eurjchem-336	122	6	64.42	64.42	NUM
eurjchem-336	122	7	;	;	PUNCT
eurjchem-336	122	8	h	h	X
eurjchem-336	122	9	,	,	PUNCT
eurjchem-336	122	10	3.69	3.69	NUM
eurjchem-336	122	11	;	;	PUNCT
eurjchem-336	122	12	n	n	CCONJ
eurjchem-336	122	13	,	,	PUNCT
eurjchem-336	122	14	9.39	9.39	NUM
eurjchem-336	122	15	.	.	PUNCT
eurjchem-336	122	16	found	find	VERB
eurjchem-336	122	17	:	:	PUNCT
eurjchem-336	123	1	c	c	X
eurjchem-336	123	2	,	,	PUNCT
eurjchem-336	123	3	63.91	63.91	NUM
eurjchem-336	123	4	;	;	PUNCT
eurjchem-336	123	5	h	h	NOUN
eurjchem-336	123	6	,	,	PUNCT
eurjchem-336	123	7	3.58	3.58	NUM
eurjchem-336	123	8	;	;	PUNCT
eurjchem-336	123	9	n	n	CCONJ
eurjchem-336	123	10	,	,	PUNCT
eurjchem-336	123	11	9.44	9.44	NUM
eurjchem-336	123	12	%	%	NOUN
eurjchem-336	123	13	.	.	PUNCT
eurjchem-336	124	1	3‐(5‐bromo‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	3‐(5‐bromo‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	NUM
eurjchem-336	124	2	carbaldehyde	carbaldehyde	NOUN
eurjchem-336	124	3	(	(	PUNCT
eurjchem-336	124	4	3b	3b	NUM
eurjchem-336	124	5	):	):	PUNCT
eurjchem-336	124	6	yield	yield	NOUN
eurjchem-336	124	7	:	:	PUNCT
eurjchem-336	124	8	86	86	NUM
eurjchem-336	124	9	%	%	NOUN
eurjchem-336	124	10	.	.	PUNCT
eurjchem-336	125	1	m.p	m.p	PROPN
eurjchem-336	125	2	.	.	PROPN
eurjchem-336	125	3	:	:	PUNCT
eurjchem-336	126	1	133‐134	133‐134	NUM
eurjchem-336	126	2	oc	oc	X
eurjchem-336	126	3	.	.	PUNCT
eurjchem-336	126	4	ft‐ir	ft‐ir	NOUN
eurjchem-336	126	5	(	(	PUNCT
eurjchem-336	126	6	kbr	kbr	PROPN
eurjchem-336	126	7	,	,	PUNCT
eurjchem-336	126	8			PROPN
eurjchem-336	126	9	,	,	PUNCT
eurjchem-336	126	10	cm‐1	cm‐1	PROPN
eurjchem-336	126	11	):	):	PUNCT
eurjchem-336	126	12	3454	3454	NUM
eurjchem-336	126	13	,	,	PUNCT
eurjchem-336	126	14	1683	1683	NUM
eurjchem-336	126	15	,	,	PUNCT
eurjchem-336	126	16	1598	1598	NUM
eurjchem-336	126	17	.	.	PUNCT
eurjchem-336	126	18	1h	1h	NUM
eurjchem-336	126	19	nmr	nmr	NOUN
eurjchem-336	126	20	(	(	PUNCT
eurjchem-336	126	21	300	300	NUM
eurjchem-336	126	22	mhz	mhz	NOUN
eurjchem-336	126	23	,	,	PUNCT
eurjchem-336	126	24	cdcl3	cdcl3	NOUN
eurjchem-336	126	25	):	):	PUNCT
eurjchem-336	126	26	7.01	7.01	NUM
eurjchem-336	126	27	(	(	PUNCT
eurjchem-336	126	28	d	d	PROPN
eurjchem-336	126	29	,	,	PUNCT
eurjchem-336	126	30	1h	1h	NUM
eurjchem-336	126	31	,	,	PUNCT
eurjchem-336	126	32	j	j	PROPN
eurjchem-336	126	33	=	=	PROPN
eurjchem-336	126	34	8.7	8.7	NUM
eurjchem-336	126	35	hz	hz	NOUN
eurjchem-336	126	36	)	)	PUNCT
eurjchem-336	126	37	,	,	PUNCT
eurjchem-336	126	38	7.42‐7.49	7.42‐7.49	NUM
eurjchem-336	126	39	(	(	PUNCT
eurjchem-336	126	40	m	m	PROPN
eurjchem-336	126	41	,	,	PUNCT
eurjchem-336	126	42	2h	2h	NUM
eurjchem-336	126	43	)	)	PUNCT
eurjchem-336	126	44	,	,	PUNCT
eurjchem-336	126	45	7.57	7.57	NUM
eurjchem-336	126	46	(	(	PUNCT
eurjchem-336	126	47	t	t	PROPN
eurjchem-336	126	48	,	,	PUNCT
eurjchem-336	126	49	2h	2h	NUM
eurjchem-336	126	50	,	,	PUNCT
eurjchem-336	126	51	j	j	PROPN
eurjchem-336	126	52	=	=	SYM
eurjchem-336	126	53	8.4hz	8.4hz	PROPN
eurjchem-336	126	54	)	)	PUNCT
eurjchem-336	126	55	,	,	PUNCT
eurjchem-336	126	56	7.72	7.72	NUM
eurjchem-336	126	57	(	(	PUNCT
eurjchem-336	126	58	d	d	PROPN
eurjchem-336	126	59	,	,	PUNCT
eurjchem-336	126	60	2h	2h	NUM
eurjchem-336	126	61	,	,	PUNCT
eurjchem-336	126	62	j	j	PROPN
eurjchem-336	126	63	=	=	PROPN
eurjchem-336	126	64	8.4	8.4	NUM
eurjchem-336	126	65	hz	hz	NOUN
eurjchem-336	126	66	)	)	PUNCT
eurjchem-336	126	67	,	,	PUNCT
eurjchem-336	126	68	8.23	8.23	NUM
eurjchem-336	126	69	(	(	PUNCT
eurjchem-336	126	70	s	s	PROPN
eurjchem-336	126	71	,	,	PUNCT
eurjchem-336	126	72	1h	1h	NUM
eurjchem-336	126	73	)	)	PUNCT
eurjchem-336	126	74	,	,	PUNCT
eurjchem-336	126	75	8.59	8.59	NUM
eurjchem-336	126	76	(	(	PUNCT
eurjchem-336	126	77	s	s	PROPN
eurjchem-336	126	78	,	,	PUNCT
eurjchem-336	126	79	1h	1h	NUM
eurjchem-336	126	80	)	)	PUNCT
eurjchem-336	126	81	,	,	PUNCT
eurjchem-336	126	82	10.18	10.18	NUM
eurjchem-336	126	83	(	(	PUNCT
eurjchem-336	126	84	s	s	PROPN
eurjchem-336	126	85	,	,	PUNCT
eurjchem-336	126	86	1h	1h	NUM
eurjchem-336	126	87	)	)	PUNCT
eurjchem-336	126	88	,	,	PUNCT
eurjchem-336	126	89	10.20	10.20	NUM
eurjchem-336	126	90	(	(	PUNCT
eurjchem-336	126	91	s	s	PROPN
eurjchem-336	126	92	,	,	PUNCT
eurjchem-336	126	93	1h	1h	NUM
eurjchem-336	126	94	)	)	PUNCT
eurjchem-336	126	95	.	.	PUNCT
eurjchem-336	126	96	13c	13c	NOUN
eurjchem-336	126	97	nmr	nmr	NOUN
eurjchem-336	126	98	(	(	PUNCT
eurjchem-336	126	99	75	75	NUM
eurjchem-336	126	100	mhz	mhz	NOUN
eurjchem-336	126	101	,	,	PUNCT
eurjchem-336	126	102	cdcl3	cdcl3	NOUN
eurjchem-336	126	103	):	):	PUNCT
eurjchem-336	126	104	117.2	117.2	NUM
eurjchem-336	126	105	,	,	PUNCT
eurjchem-336	126	106	117.7	117.7	NUM
eurjchem-336	126	107	,	,	PUNCT
eurjchem-336	126	108	118.0	118.0	NUM
eurjchem-336	126	109	,	,	PUNCT
eurjchem-336	126	110	119.2	119.2	NUM
eurjchem-336	126	111	,	,	PUNCT
eurjchem-336	126	112	124.8	124.8	NUM
eurjchem-336	126	113	,	,	PUNCT
eurjchem-336	126	114	128.4	128.4	NUM
eurjchem-336	126	115	,	,	PUNCT
eurjchem-336	126	116	131.2	131.2	NUM
eurjchem-336	126	117	,	,	PUNCT
eurjchem-336	126	118	131.4	131.4	NUM
eurjchem-336	126	119	,	,	PUNCT
eurjchem-336	126	120	133.7	133.7	NUM
eurjchem-336	126	121	,	,	PUNCT
eurjchem-336	126	122	134.6	134.6	NUM
eurjchem-336	126	123	,	,	PUNCT
eurjchem-336	126	124	141.8	141.8	NUM
eurjchem-336	126	125	,	,	PUNCT
eurjchem-336	126	126	151.8	151.8	NUM
eurjchem-336	126	127	,	,	PUNCT
eurjchem-336	126	128	153.6	153.6	NUM
eurjchem-336	126	129	,	,	PUNCT
eurjchem-336	126	130	183.4	183.4	NUM
eurjchem-336	126	131	.	.	PUNCT
eurjchem-336	127	1	ms	ms	NOUN
eurjchem-336	127	2	(	(	PUNCT
eurjchem-336	127	3	ei	ei	PROPN
eurjchem-336	127	4	,	,	PUNCT
eurjchem-336	127	5	m	m	PROPN
eurjchem-336	127	6	/	/	SYM
eurjchem-336	127	7	z	z	NOUN
eurjchem-336	127	8	):	):	PUNCT
eurjchem-336	127	9	342	342	NUM
eurjchem-336	127	10	(	(	PUNCT
eurjchem-336	127	11	m+	m+	NUM
eurjchem-336	127	12	)	)	PUNCT
eurjchem-336	127	13	.	.	PUNCT
eurjchem-336	128	1	anal	anal	PROPN
eurjchem-336	128	2	.	.	PUNCT
eurjchem-336	128	3	calcd	calcd	NOUN
eurjchem-336	128	4	.	.	PUNCT
eurjchem-336	129	1	for	for	ADP
eurjchem-336	129	2	c16h11n2o2br	c16h11n2o2br	PROPN
eurjchem-336	129	3	:	:	PUNCT
eurjchem-336	129	4	c	c	X
eurjchem-336	129	5	,	,	PUNCT
eurjchem-336	129	6	56.14	56.14	NUM
eurjchem-336	129	7	;	;	PUNCT
eurjchem-336	129	8	h	h	NOUN
eurjchem-336	129	9	,	,	PUNCT
eurjchem-336	129	10	3.21	3.21	NUM
eurjchem-336	129	11	;	;	PUNCT
eurjchem-336	129	12	n	n	CCONJ
eurjchem-336	129	13	,	,	PUNCT
eurjchem-336	129	14	8.18	8.18	NUM
eurjchem-336	129	15	.	.	PUNCT
eurjchem-336	129	16	found	find	VERB
eurjchem-336	129	17	:	:	PUNCT
eurjchem-336	130	1	c	c	X
eurjchem-336	130	2	,	,	PUNCT
eurjchem-336	130	3	56.23	56.23	NUM
eurjchem-336	130	4	;	;	PUNCT
eurjchem-336	130	5	h	h	NOUN
eurjchem-336	130	6	,	,	PUNCT
eurjchem-336	130	7	3.28	3.28	NUM
eurjchem-336	130	8	;	;	PUNCT
eurjchem-336	130	9	n	n	CCONJ
eurjchem-336	130	10	,	,	PUNCT
eurjchem-336	130	11	8.23	8.23	NUM
eurjchem-336	130	12	%	%	NOUN
eurjchem-336	130	13	.	.	PUNCT
eurjchem-336	131	1	3‐(3‐chloro‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	3‐(3‐chloro‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	NUM
eurjchem-336	131	2	carbaldehyde	carbaldehyde	NOUN
eurjchem-336	131	3	(	(	PUNCT
eurjchem-336	131	4	3c	3c	NUM
eurjchem-336	131	5	):	):	PUNCT
eurjchem-336	131	6	yield	yield	NOUN
eurjchem-336	131	7	:	:	PUNCT
eurjchem-336	131	8	85	85	NUM
eurjchem-336	131	9	%	%	NOUN
eurjchem-336	131	10	.	.	PUNCT
eurjchem-336	132	1	m.p	m.p	PROPN
eurjchem-336	132	2	.	.	PROPN
eurjchem-336	132	3	:	:	PUNCT
eurjchem-336	133	1	149‐150	149‐150	NUM
eurjchem-336	133	2	oc	oc	NOUN
eurjchem-336	133	3	.	.	PUNCT
eurjchem-336	133	4	ft‐ir	ft‐ir	NOUN
eurjchem-336	133	5	(	(	PUNCT
eurjchem-336	133	6	kbr	kbr	PROPN
eurjchem-336	133	7	,	,	PUNCT
eurjchem-336	133	8			PROPN
eurjchem-336	133	9	,	,	PUNCT
eurjchem-336	133	10	cm‐1	cm‐1	PROPN
eurjchem-336	133	11	):	):	PUNCT
eurjchem-336	133	12	3448	3448	NUM
eurjchem-336	133	13	,	,	PUNCT
eurjchem-336	133	14	1693	1693	NUM
eurjchem-336	133	15	,	,	PUNCT
eurjchem-336	133	16	1664	1664	NUM
eurjchem-336	133	17	.	.	PUNCT
eurjchem-336	134	1	1h	1h	NUM
eurjchem-336	134	2	nmr	nmr	NOUN
eurjchem-336	134	3	(	(	PUNCT
eurjchem-336	134	4	300	300	NUM
eurjchem-336	134	5	mhz	mhz	NOUN
eurjchem-336	134	6	,	,	PUNCT
eurjchem-336	134	7	cdcl3	cdcl3	NOUN
eurjchem-336	134	8	):	):	PUNCT
eurjchem-336	134	9	6.97	6.97	NUM
eurjchem-336	134	10	(	(	PUNCT
eurjchem-336	134	11	t	t	PROPN
eurjchem-336	134	12	,	,	PUNCT
eurjchem-336	134	13	1h	1h	NUM
eurjchem-336	134	14	,	,	PUNCT
eurjchem-336	134	15	j	j	PROPN
eurjchem-336	134	16	=	=	SYM
eurjchem-336	134	17	7.8	7.8	NUM
eurjchem-336	134	18	hz	hz	NOUN
eurjchem-336	134	19	)	)	PUNCT
eurjchem-336	134	20	,	,	PUNCT
eurjchem-336	134	21	7.41‐7.45	7.41‐7.45	NUM
eurjchem-336	134	22	(	(	PUNCT
eurjchem-336	134	23	m	m	PROPN
eurjchem-336	134	24	,	,	PUNCT
eurjchem-336	134	25	2h	2h	NUM
eurjchem-336	134	26	)	)	PUNCT
eurjchem-336	134	27	,	,	PUNCT
eurjchem-336	134	28	7.53	7.53	NUM
eurjchem-336	134	29	(	(	PUNCT
eurjchem-336	134	30	t	t	PROPN
eurjchem-336	134	31	,	,	PUNCT
eurjchem-336	134	32	2h	2h	NUM
eurjchem-336	134	33	,	,	PUNCT
eurjchem-336	134	34	j	j	PROPN
eurjchem-336	134	35	=	=	SYM
eurjchem-336	134	36	7.5	7.5	NUM
eurjchem-336	134	37	hz	hz	NOUN
eurjchem-336	134	38	)	)	PUNCT
eurjchem-336	134	39	,	,	PUNCT
eurjchem-336	134	40	7.71	7.71	NUM
eurjchem-336	134	41	(	(	PUNCT
eurjchem-336	134	42	d	d	NOUN
eurjchem-336	134	43	,	,	PUNCT
eurjchem-336	134	44	2h	2h	NUM
eurjchem-336	134	45	,	,	PUNCT
eurjchem-336	134	46	j	j	PROPN
eurjchem-336	134	47	=	=	SYM
eurjchem-336	134	48	8.1	8.1	NUM
eurjchem-336	134	49	hz	hz	NOUN
eurjchem-336	134	50	)	)	PUNCT
eurjchem-336	134	51	,	,	PUNCT
eurjchem-336	134	52	7.98	7.98	NUM
eurjchem-336	134	53	(	(	PUNCT
eurjchem-336	134	54	d	d	PROPN
eurjchem-336	134	55	,	,	PUNCT
eurjchem-336	134	56	1h	1h	NUM
eurjchem-336	134	57	,	,	PUNCT
eurjchem-336	134	58	j	j	PROPN
eurjchem-336	135	1	=	=	SYM
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eurjchem-336	135	3	hz	hz	NOUN
eurjchem-336	135	4	)	)	PUNCT
eurjchem-336	135	5	,	,	PUNCT
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eurjchem-336	135	7	(	(	PUNCT
eurjchem-336	135	8	s	s	PROPN
eurjchem-336	135	9	,	,	PUNCT
eurjchem-336	135	10	1h	1h	NUM
eurjchem-336	135	11	)	)	PUNCT
eurjchem-336	135	12	,	,	PUNCT
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eurjchem-336	135	14	(	(	PUNCT
eurjchem-336	135	15	s	s	PROPN
eurjchem-336	135	16	,	,	PUNCT
eurjchem-336	135	17	1h	1h	NUM
eurjchem-336	135	18	)	)	PUNCT
eurjchem-336	135	19	,	,	PUNCT
eurjchem-336	135	20	10.65	10.65	NUM
eurjchem-336	135	21	(	(	PUNCT
eurjchem-336	135	22	s	s	PROPN
eurjchem-336	135	23	,	,	PUNCT
eurjchem-336	135	24	1h	1h	NUM
eurjchem-336	135	25	)	)	PUNCT
eurjchem-336	135	26	.	.	PUNCT
eurjchem-336	136	1	13c	13c	NOUN
eurjchem-336	136	2	nmr	nmr	NOUN
eurjchem-336	136	3	(	(	PUNCT
eurjchem-336	136	4	75	75	NUM
eurjchem-336	136	5	mhz	mhz	NOUN
eurjchem-336	136	6	,	,	PUNCT
eurjchem-336	136	7	cdcl3	cdcl3	NOUN
eurjchem-336	136	8	):	):	PUNCT
eurjchem-336	136	9	116.6	116.6	NUM
eurjchem-336	136	10	,	,	PUNCT
eurjchem-336	136	11	119.2	119.2	NUM
eurjchem-336	136	12	,	,	PUNCT
eurjchem-336	136	13	119.5	119.5	NUM
eurjchem-336	136	14	,	,	PUNCT
eurjchem-336	136	15	121.9	121.9	NUM
eurjchem-336	136	16	,	,	PUNCT
eurjchem-336	136	17	123.0	123.0	NUM
eurjchem-336	136	18	,	,	PUNCT
eurjchem-336	136	19	128.2	128.2	NUM
eurjchem-336	136	20	,	,	PUNCT
eurjchem-336	136	21	128.4	128.4	NUM
eurjchem-336	136	22	,	,	PUNCT
eurjchem-336	136	23	129.8	129.8	NUM
eurjchem-336	136	24	,	,	PUNCT
eurjchem-336	136	25	131.2	131.2	NUM
eurjchem-336	136	26	,	,	PUNCT
eurjchem-336	136	27	133.4	133.4	NUM
eurjchem-336	136	28	,	,	PUNCT
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eurjchem-336	136	30	,	,	PUNCT
eurjchem-336	136	31	151.4	151.4	NUM
eurjchem-336	136	32	,	,	PUNCT
eurjchem-336	136	33	151.7	151.7	NUM
eurjchem-336	136	34	,	,	PUNCT
eurjchem-336	136	35	183.5	183.5	NUM
eurjchem-336	136	36	.	.	PUNCT
eurjchem-336	137	1	ms	ms	NOUN
eurjchem-336	137	2	(	(	PUNCT
eurjchem-336	137	3	ei	ei	PROPN
eurjchem-336	137	4	,	,	PUNCT
eurjchem-336	137	5	m	m	PROPN
eurjchem-336	137	6	/	/	SYM
eurjchem-336	137	7	z	z	PROPN
eurjchem-336	137	8	):	):	PUNCT
eurjchem-336	137	9	298	298	NUM
eurjchem-336	137	10	(	(	PUNCT
eurjchem-336	137	11	m+	m+	NUM
eurjchem-336	137	12	)	)	PUNCT
eurjchem-336	137	13	.	.	PUNCT
eurjchem-336	138	1	anal	anal	PROPN
eurjchem-336	138	2	.	.	PUNCT
eurjchem-336	138	3	calcd	calcd	NOUN
eurjchem-336	138	4	.	.	PUNCT
eurjchem-336	139	1	for	for	SCONJ
eurjchem-336	139	2	c16h11n2o2cl	c16h11n2o2cl	PROPN
eurjchem-336	139	3	:	:	PUNCT
eurjchem-336	139	4	c	c	X
eurjchem-336	139	5	,	,	PUNCT
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eurjchem-336	139	7	;	;	PUNCT
eurjchem-336	139	8	h	h	X
eurjchem-336	139	9	,	,	PUNCT
eurjchem-336	139	10	3.69	3.69	NUM
eurjchem-336	139	11	;	;	PUNCT
eurjchem-336	139	12	n	n	CCONJ
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eurjchem-336	139	17	:	:	PUNCT
eurjchem-336	140	1	c	c	X
eurjchem-336	140	2	,	,	PUNCT
eurjchem-336	140	3	64.65	64.65	NUM
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eurjchem-336	140	5	h	h	NOUN
eurjchem-336	140	6	,	,	PUNCT
eurjchem-336	140	7	3.74	3.74	NUM
eurjchem-336	140	8	;	;	PUNCT
eurjchem-336	140	9	n	n	CCONJ
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eurjchem-336	140	11	9.33	9.33	NUM
eurjchem-336	140	12	%	%	NOUN
eurjchem-336	140	13	.	.	PUNCT
eurjchem-336	141	1	3‐(3,5‐dichloro‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	3‐(3,5‐dichloro‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	NUM
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eurjchem-336	141	3	(	(	PUNCT
eurjchem-336	141	4	3d	3d	NOUN
eurjchem-336	141	5	):	):	PUNCT
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eurjchem-336	141	7	:	:	PUNCT
eurjchem-336	141	8	88	88	NUM
eurjchem-336	141	9	%	%	NOUN
eurjchem-336	141	10	.	.	PUNCT
eurjchem-336	142	1	m.p	m.p	PROPN
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eurjchem-336	142	3	:	:	PUNCT
eurjchem-336	143	1	166‐167	166‐167	NUM
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eurjchem-336	143	3	.	.	PUNCT
eurjchem-336	143	4	ft‐ir	ft‐ir	NOUN
eurjchem-336	143	5	(	(	PUNCT
eurjchem-336	143	6	kbr	kbr	PROPN
eurjchem-336	143	7	,	,	PUNCT
eurjchem-336	143	8			PROPN
eurjchem-336	143	9	,	,	PUNCT
eurjchem-336	143	10	cm‐1	cm‐1	PROPN
eurjchem-336	143	11	):	):	PUNCT
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eurjchem-336	143	13	,	,	PUNCT
eurjchem-336	143	14	1687	1687	NUM
eurjchem-336	143	15	,	,	PUNCT
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eurjchem-336	143	17	.	.	PUNCT
eurjchem-336	144	1	1h	1h	NUM
eurjchem-336	144	2	nmr	nmr	NOUN
eurjchem-336	144	3	(	(	PUNCT
eurjchem-336	144	4	300	300	NUM
eurjchem-336	144	5	mhz	mhz	NOUN
eurjchem-336	144	6	,	,	PUNCT
eurjchem-336	144	7	cdcl3	cdcl3	NOUN
eurjchem-336	144	8	):	):	PUNCT
eurjchem-336	144	9	7.44‐7.47	7.44‐7.47	PROPN
eurjchem-336	144	10	(	(	PUNCT
eurjchem-336	144	11	m	m	PROPN
eurjchem-336	144	12	,	,	PUNCT
eurjchem-336	144	13	2h	2h	NUM
eurjchem-336	144	14	)	)	PUNCT
eurjchem-336	144	15	,	,	PUNCT
eurjchem-336	144	16	7.54	7.54	NUM
eurjchem-336	144	17	(	(	PUNCT
eurjchem-336	144	18	t	t	PROPN
eurjchem-336	144	19	,	,	PUNCT
eurjchem-336	144	20	2h	2h	NUM
eurjchem-336	144	21	,	,	PUNCT
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eurjchem-336	144	23	=	=	SYM
eurjchem-336	144	24	7.5hz	7.5hz	PROPN
eurjchem-336	144	25	)	)	PUNCT
eurjchem-336	144	26	,	,	PUNCT
eurjchem-336	144	27	7.70	7.70	NUM
eurjchem-336	144	28	(	(	PUNCT
eurjchem-336	144	29	d	d	PROPN
eurjchem-336	144	30	,	,	PUNCT
eurjchem-336	144	31	2h	2h	NUM
eurjchem-336	144	32	,	,	PUNCT
eurjchem-336	144	33	j	j	PROPN
eurjchem-336	144	34	=	=	SYM
eurjchem-336	144	35	7.5	7.5	NUM
eurjchem-336	144	36	hz	hz	NOUN
eurjchem-336	144	37	)	)	PUNCT
eurjchem-336	144	38	,	,	PUNCT
eurjchem-336	144	39	8.18	8.18	NUM
eurjchem-336	144	40	(	(	PUNCT
eurjchem-336	144	41	s	s	PROPN
eurjchem-336	144	42	,	,	PUNCT
eurjchem-336	144	43	1h	1h	NUM
eurjchem-336	144	44	)	)	PUNCT
eurjchem-336	144	45	,	,	PUNCT
eurjchem-336	144	46	8.54	8.54	NUM
eurjchem-336	144	47	(	(	PUNCT
eurjchem-336	144	48	s	s	PROPN
eurjchem-336	144	49	,	,	PUNCT
eurjchem-336	144	50	1h	1h	NUM
eurjchem-336	144	51	)	)	PUNCT
eurjchem-336	144	52	,	,	PUNCT
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eurjchem-336	144	54	(	(	PUNCT
eurjchem-336	144	55	s	s	PROPN
eurjchem-336	144	56	,	,	PUNCT
eurjchem-336	144	57	1h	1h	NUM
eurjchem-336	144	58	)	)	PUNCT
eurjchem-336	144	59	,	,	PUNCT
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eurjchem-336	144	61	(	(	PUNCT
eurjchem-336	144	62	s	s	PROPN
eurjchem-336	144	63	,	,	PUNCT
eurjchem-336	144	64	1h	1h	NUM
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eurjchem-336	144	66	.	.	PUNCT
eurjchem-336	145	1	13c	13c	NOUN
eurjchem-336	145	2	nmr	nmr	NOUN
eurjchem-336	145	3	(	(	PUNCT
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eurjchem-336	145	5	mhz	mhz	NOUN
eurjchem-336	145	6	,	,	PUNCT
eurjchem-336	145	7	cdcl3	cdcl3	NOUN
eurjchem-336	145	8	):	):	PUNCT
eurjchem-336	145	9	117.4	117.4	NUM
eurjchem-336	145	10	,	,	PUNCT
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eurjchem-336	145	12	,	,	PUNCT
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eurjchem-336	145	14	,	,	PUNCT
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eurjchem-336	145	16	,	,	PUNCT
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eurjchem-336	145	18	,	,	PUNCT
eurjchem-336	145	19	127.9	127.9	NUM
eurjchem-336	145	20	,	,	PUNCT
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eurjchem-336	145	22	,	,	PUNCT
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eurjchem-336	145	24	,	,	PUNCT
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eurjchem-336	145	26	,	,	PUNCT
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eurjchem-336	145	28	,	,	PUNCT
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eurjchem-336	145	30	,	,	PUNCT
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eurjchem-336	145	32	,	,	PUNCT
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eurjchem-336	145	34	,	,	PUNCT
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eurjchem-336	145	36	.	.	PUNCT
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eurjchem-336	146	2	(	(	PUNCT
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eurjchem-336	146	4	,	,	PUNCT
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eurjchem-336	146	7	z	z	PROPN
eurjchem-336	146	8	):	):	PUNCT
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eurjchem-336	146	10	(	(	PUNCT
eurjchem-336	146	11	m+	m+	NUM
eurjchem-336	146	12	)	)	PUNCT
eurjchem-336	146	13	.	.	PUNCT
eurjchem-336	147	1	anal	anal	PROPN
eurjchem-336	147	2	.	.	PUNCT
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eurjchem-336	147	4	.	.	PUNCT
eurjchem-336	148	1	for	for	ADP
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eurjchem-336	148	3	:	:	PUNCT
eurjchem-336	148	4	c	c	X
eurjchem-336	148	5	,	,	PUNCT
eurjchem-336	148	6	57.83	57.83	NUM
eurjchem-336	148	7	;	;	PUNCT
eurjchem-336	148	8	h	h	X
eurjchem-336	148	9	,	,	PUNCT
eurjchem-336	148	10	3.01	3.01	NUM
eurjchem-336	148	11	;	;	PUNCT
eurjchem-336	148	12	n	n	CCONJ
eurjchem-336	148	13	,	,	PUNCT
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eurjchem-336	148	17	:	:	PUNCT
eurjchem-336	148	18	c	c	X
eurjchem-336	148	19	,	,	PUNCT
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eurjchem-336	148	21	;	;	PUNCT
eurjchem-336	148	22	h	h	NOUN
eurjchem-336	148	23	,	,	PUNCT
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eurjchem-336	148	25	;	;	PUNCT
eurjchem-336	148	26	n	n	CCONJ
eurjchem-336	148	27	,	,	PUNCT
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eurjchem-336	148	30	.	.	PUNCT
eurjchem-336	149	1	3‐(3,5‐dibromo‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	3‐(3,5‐dibromo‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	NUM
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eurjchem-336	149	3	(	(	PUNCT
eurjchem-336	149	4	3e	3e	NUM
eurjchem-336	149	5	):	):	PUNCT
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eurjchem-336	149	7	:	:	PUNCT
eurjchem-336	149	8	87	87	NUM
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eurjchem-336	149	10	.	.	PUNCT
eurjchem-336	150	1	m.p	m.p	PROPN
eurjchem-336	150	2	.	.	PROPN
eurjchem-336	150	3	:	:	PUNCT
eurjchem-336	151	1	172‐173	172‐173	NUM
eurjchem-336	151	2	oc	oc	NOUN
eurjchem-336	151	3	.	.	PUNCT
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eurjchem-336	151	5	(	(	PUNCT
eurjchem-336	151	6	kbr	kbr	PROPN
eurjchem-336	151	7	,	,	PUNCT
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eurjchem-336	151	9	,	,	PUNCT
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eurjchem-336	151	17	.	.	PUNCT
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eurjchem-336	152	3	(	(	PUNCT
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eurjchem-336	152	6	,	,	PUNCT
eurjchem-336	152	7	cdcl3	cdcl3	NOUN
eurjchem-336	152	8	):	):	PUNCT
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eurjchem-336	152	11	t	t	PROPN
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eurjchem-336	152	14	,	,	PUNCT
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eurjchem-336	152	16	=	=	SYM
eurjchem-336	152	17	8.7hz	8.7hz	PROPN
eurjchem-336	152	18	)	)	PUNCT
eurjchem-336	152	19	,	,	PUNCT
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eurjchem-336	152	21	(	(	PUNCT
eurjchem-336	152	22	t	t	PROPN
eurjchem-336	152	23	,	,	PUNCT
eurjchem-336	152	24	2h	2h	NUM
eurjchem-336	152	25	,	,	PUNCT
eurjchem-336	152	26	j	j	PROPN
eurjchem-336	152	27	=	=	PROPN
eurjchem-336	152	28	8.7	8.7	NUM
eurjchem-336	152	29	hz	hz	NOUN
eurjchem-336	152	30	)	)	PUNCT
eurjchem-336	152	31	,	,	PUNCT
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eurjchem-336	152	33	(	(	PUNCT
eurjchem-336	152	34	d	d	PROPN
eurjchem-336	152	35	,	,	PUNCT
eurjchem-336	152	36	2h	2h	NUM
eurjchem-336	152	37	,	,	PUNCT
eurjchem-336	152	38	j	j	PROPN
eurjchem-336	152	39	=	=	PROPN
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eurjchem-336	152	41	hz	hz	NOUN
eurjchem-336	152	42	)	)	PUNCT
eurjchem-336	152	43	,	,	PUNCT
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eurjchem-336	152	45	(	(	PUNCT
eurjchem-336	152	46	d	d	PROPN
eurjchem-336	152	47	,	,	PUNCT
eurjchem-336	152	48	1h	1h	NUM
eurjchem-336	152	49	,	,	PUNCT
eurjchem-336	152	50	j	j	PROPN
eurjchem-336	152	51	=	=	SYM
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eurjchem-336	152	53	hz	hz	NOUN
eurjchem-336	152	54	)	)	PUNCT
eurjchem-336	152	55	,	,	PUNCT
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eurjchem-336	152	58	d	d	PROPN
eurjchem-336	152	59	,	,	PUNCT
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eurjchem-336	152	63	=	=	SYM
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eurjchem-336	152	65	hz	hz	NOUN
eurjchem-336	152	66	)	)	PUNCT
eurjchem-336	152	67	,	,	PUNCT
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eurjchem-336	152	71	,	,	PUNCT
eurjchem-336	152	72	1h	1h	NUM
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eurjchem-336	152	74	,	,	PUNCT
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eurjchem-336	153	3	(	(	PUNCT
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eurjchem-336	153	6	,	,	PUNCT
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eurjchem-336	153	8	):	):	PUNCT
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eurjchem-336	153	18	,	,	PUNCT
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eurjchem-336	153	20	,	,	PUNCT
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eurjchem-336	153	22	,	,	PUNCT
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eurjchem-336	153	24	,	,	PUNCT
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eurjchem-336	153	26	,	,	PUNCT
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eurjchem-336	153	28	,	,	PUNCT
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eurjchem-336	153	30	,	,	PUNCT
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eurjchem-336	153	32	,	,	PUNCT
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eurjchem-336	153	36	.	.	PUNCT
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eurjchem-336	154	2	(	(	PUNCT
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eurjchem-336	154	7	z	z	NOUN
eurjchem-336	154	8	):	):	PUNCT
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eurjchem-336	154	10	(	(	PUNCT
eurjchem-336	154	11	m+4	m+4	PROPN
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eurjchem-336	154	13	,	,	PUNCT
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eurjchem-336	154	15	(	(	PUNCT
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eurjchem-336	154	17	)	)	PUNCT
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eurjchem-336	154	29	2	2	NUM
eurjchem-336	154	30	(	(	PUNCT
eurjchem-336	154	31	2	2	NUM
eurjchem-336	154	32	)	)	PUNCT
eurjchem-336	154	33	(	(	PUNCT
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eurjchem-336	154	35	)	)	PUNCT
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eurjchem-336	154	37	225	225	NUM
eurjchem-336	154	38	(	(	PUNCT
eurjchem-336	154	39	m+	m+	NUM
eurjchem-336	154	40	)	)	PUNCT
eurjchem-336	154	41	.	.	PUNCT
eurjchem-336	155	1	anal	anal	PROPN
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eurjchem-336	155	4	.	.	PUNCT
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eurjchem-336	156	5	,	,	PUNCT
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eurjchem-336	156	8	h	h	NOUN
eurjchem-336	156	9	,	,	PUNCT
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eurjchem-336	156	11	;	;	PUNCT
eurjchem-336	156	12	n	n	CCONJ
eurjchem-336	156	13	,	,	PUNCT
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eurjchem-336	156	17	:	:	PUNCT
eurjchem-336	157	1	c	c	X
eurjchem-336	157	2	,	,	PUNCT
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eurjchem-336	157	4	;	;	PUNCT
eurjchem-336	157	5	h	h	NOUN
eurjchem-336	157	6	,	,	PUNCT
eurjchem-336	157	7	2.35	2.35	NUM
eurjchem-336	157	8	;	;	PUNCT
eurjchem-336	157	9	n	n	CCONJ
eurjchem-336	157	10	,	,	PUNCT
eurjchem-336	157	11	6.71	6.71	NUM
eurjchem-336	157	12	%	%	NOUN
eurjchem-336	157	13	.	.	PUNCT
eurjchem-336	158	1	3‐(3‐bromo‐5‐chloro‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐	3‐(3‐bromo‐5‐chloro‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐	NUM
eurjchem-336	158	2	pyrazole‐4‐carbaldehyde	pyrazole‐4‐carbaldehyde	NUM
eurjchem-336	158	3	(	(	PUNCT
eurjchem-336	158	4	3f	3f	NUM
eurjchem-336	158	5	):	):	PUNCT
eurjchem-336	158	6	yield	yield	NOUN
eurjchem-336	158	7	:	:	PUNCT
eurjchem-336	158	8	84	84	NUM
eurjchem-336	158	9	%	%	NOUN
eurjchem-336	158	10	.	.	PUNCT
eurjchem-336	159	1	m.p	m.p	PROPN
eurjchem-336	159	2	.	.	PROPN
eurjchem-336	159	3	:	:	PUNCT
eurjchem-336	160	1	175‐176	175‐176	PROPN
eurjchem-336	160	2	oc	oc	AUX
eurjchem-336	160	3	.	.	PUNCT
eurjchem-336	160	4	ft‐	ft‐	PROPN
eurjchem-336	160	5	ir	ir	PROPN
eurjchem-336	160	6	(	(	PUNCT
eurjchem-336	160	7	kbr	kbr	PROPN
eurjchem-336	160	8	,	,	PUNCT
eurjchem-336	160	9			PROPN
eurjchem-336	160	10	,	,	PUNCT
eurjchem-336	160	11	cm‐1	cm‐1	PROPN
eurjchem-336	160	12	):	):	PUNCT
eurjchem-336	160	13	3344	3344	NUM
eurjchem-336	160	14	,	,	PUNCT
eurjchem-336	160	15	1685	1685	NUM
eurjchem-336	160	16	,	,	PUNCT
eurjchem-336	160	17	1649	1649	NUM
eurjchem-336	160	18	.	.	PUNCT
eurjchem-336	161	1	1h	1h	NUM
eurjchem-336	161	2	nmr	nmr	NOUN
eurjchem-336	161	3	(	(	PUNCT
eurjchem-336	161	4	300	300	NUM
eurjchem-336	161	5	mhz	mhz	NOUN
eurjchem-336	161	6	,	,	PUNCT
eurjchem-336	161	7	cdcl3	cdcl3	NOUN
eurjchem-336	161	8	):	):	PUNCT
eurjchem-336	161	9	7.48	7.48	NUM
eurjchem-336	161	10	(	(	PUNCT
eurjchem-336	161	11	t	t	PROPN
eurjchem-336	161	12	,	,	PUNCT
eurjchem-336	161	13	1h	1h	NUM
eurjchem-336	161	14	,	,	PUNCT
eurjchem-336	161	15	j	j	PROPN
eurjchem-336	161	16	=	=	SYM
eurjchem-336	161	17	7.2	7.2	NUM
eurjchem-336	161	18	hz	hz	NOUN
eurjchem-336	161	19	)	)	PUNCT
eurjchem-336	161	20	,	,	PUNCT
eurjchem-336	161	21	7.57	7.57	NUM
eurjchem-336	161	22	(	(	PUNCT
eurjchem-336	161	23	t	t	PROPN
eurjchem-336	161	24	,	,	PUNCT
eurjchem-336	161	25	2h	2h	NUM
eurjchem-336	161	26	,	,	PUNCT
eurjchem-336	161	27	j	j	PROPN
eurjchem-336	161	28	=	=	SYM
eurjchem-336	161	29	7.2	7.2	NUM
eurjchem-336	161	30	hz	hz	NOUN
eurjchem-336	161	31	)	)	PUNCT
eurjchem-336	161	32	,	,	PUNCT
eurjchem-336	161	33	7.59	7.59	NUM
eurjchem-336	161	34	(	(	PUNCT
eurjchem-336	161	35	d	d	PROPN
eurjchem-336	161	36	,	,	PUNCT
eurjchem-336	161	37	1h	1h	NUM
eurjchem-336	161	38	,	,	PUNCT
eurjchem-336	161	39	j	j	PROPN
eurjchem-336	161	40	=	=	SYM
eurjchem-336	161	41	2.4	2.4	NUM
eurjchem-336	161	42	hz	hz	NOUN
eurjchem-336	161	43	)	)	PUNCT
eurjchem-336	161	44	,	,	PUNCT
eurjchem-336	161	45	7.74	7.74	NUM
eurjchem-336	161	46	(	(	PUNCT
eurjchem-336	161	47	d	d	PROPN
eurjchem-336	161	48	,	,	PUNCT
eurjchem-336	161	49	2h	2h	NUM
eurjchem-336	161	50	,	,	PUNCT
eurjchem-336	161	51	j	j	PROPN
eurjchem-336	161	52	=	=	SYM
eurjchem-336	161	53	7.2	7.2	NUM
eurjchem-336	161	54	hz	hz	NOUN
eurjchem-336	161	55	)	)	PUNCT
eurjchem-336	161	56	,	,	PUNCT
eurjchem-336	161	57	8.26	8.26	NUM
eurjchem-336	161	58	(	(	PUNCT
eurjchem-336	161	59	d	d	PROPN
eurjchem-336	161	60	,	,	PUNCT
eurjchem-336	161	61	1h	1h	NUM
eurjchem-336	161	62	,	,	PUNCT
eurjchem-336	161	63	j	j	PROPN
eurjchem-336	161	64	=	=	SYM
eurjchem-336	161	65	2.4	2.4	NUM
eurjchem-336	161	66	hz	hz	NOUN
eurjchem-336	161	67	)	)	PUNCT
eurjchem-336	161	68	,	,	PUNCT
eurjchem-336	161	69	8.61	8.61	NUM
eurjchem-336	161	70	(	(	PUNCT
eurjchem-336	161	71	s	s	PROPN
eurjchem-336	161	72	,	,	PUNCT
eurjchem-336	161	73	1h	1h	NUM
eurjchem-336	161	74	)	)	PUNCT
eurjchem-336	161	75	,	,	PUNCT
eurjchem-336	161	76	10.16	10.16	NUM
eurjchem-336	161	77	(	(	PUNCT
eurjchem-336	161	78	s	s	PROPN
eurjchem-336	161	79	,	,	PUNCT
eurjchem-336	161	80	1h	1h	NUM
eurjchem-336	161	81	)	)	PUNCT
eurjchem-336	161	82	,	,	PUNCT
eurjchem-336	161	83	10.96	10.96	NUM
eurjchem-336	161	84	(	(	PUNCT
eurjchem-336	161	85	s	s	PROPN
eurjchem-336	161	86	,	,	PUNCT
eurjchem-336	161	87	1h	1h	NUM
eurjchem-336	161	88	)	)	PUNCT
eurjchem-336	161	89	.	.	PUNCT
eurjchem-336	162	1	13c	13c	NOUN
eurjchem-336	162	2	nmr	nmr	NOUN
eurjchem-336	162	3	(	(	PUNCT
eurjchem-336	162	4	75	75	NUM
eurjchem-336	162	5	mhz	mhz	NOUN
eurjchem-336	162	6	,	,	PUNCT
eurjchem-336	162	7	cdcl3	cdcl3	NOUN
eurjchem-336	162	8	):	):	PUNCT
eurjchem-336	162	9	117.2	117.2	NUM
eurjchem-336	162	10	,	,	PUNCT
eurjchem-336	162	11	117.6	117.6	NUM
eurjchem-336	162	12	,	,	PUNCT
eurjchem-336	162	13	119.2	119.2	NUM
eurjchem-336	162	14	,	,	PUNCT
eurjchem-336	162	15	125.2	125.2	NUM
eurjchem-336	162	16	,	,	PUNCT
eurjchem-336	162	17	128.4	128.4	NUM
eurjchem-336	162	18	,	,	PUNCT
eurjchem-336	162	19	129.3	129.3	NUM
eurjchem-336	162	20	,	,	PUNCT
eurjchem-336	162	21	131.4	131.4	NUM
eurjchem-336	162	22	,	,	PUNCT
eurjchem-336	162	23	131.6	131.6	NUM
eurjchem-336	162	24	,	,	PUNCT
eurjchem-336	162	25	132.1	132.1	NUM
eurjchem-336	162	26	,	,	PUNCT
eurjchem-336	162	27	132.9	132.9	NUM
eurjchem-336	162	28	,	,	PUNCT
eurjchem-336	162	29	139.7	139.7	NUM
eurjchem-336	162	30	,	,	PUNCT
eurjchem-336	162	31	152.5	152.5	NUM
eurjchem-336	162	32	,	,	PUNCT
eurjchem-336	162	33	154.7	154.7	NUM
eurjchem-336	162	34	,	,	PUNCT
eurjchem-336	162	35	184.1	184.1	NUM
eurjchem-336	162	36	.	.	PUNCT
eurjchem-336	163	1	ms	ms	NOUN
eurjchem-336	163	2	(	(	PUNCT
eurjchem-336	163	3	ei	ei	PROPN
eurjchem-336	163	4	,	,	PUNCT
eurjchem-336	163	5	m	m	PROPN
eurjchem-336	163	6	/	/	SYM
eurjchem-336	163	7	z	z	NOUN
eurjchem-336	163	8	):	):	PUNCT
eurjchem-336	163	9	380	380	NUM
eurjchem-336	163	10	(	(	PUNCT
eurjchem-336	163	11	m+4	m+4	PROPN
eurjchem-336	163	12	)	)	PUNCT
eurjchem-336	163	13	,	,	PUNCT
eurjchem-336	163	14	376	376	NUM
eurjchem-336	163	15	(	(	PUNCT
eurjchem-336	163	16	m+	m+	NUM
eurjchem-336	163	17	)	)	PUNCT
eurjchem-336	163	18	.	.	PUNCT
eurjchem-336	164	1	anal	anal	PROPN
eurjchem-336	164	2	.	.	PUNCT
eurjchem-336	164	3	calcd	calcd	NOUN
eurjchem-336	164	4	.	.	PUNCT
eurjchem-336	165	1	for	for	ADP
eurjchem-336	165	2	c16h10n2o2brcl	c16h10n2o2brcl	NOUN
eurjchem-336	165	3	:	:	PUNCT
eurjchem-336	165	4	c	c	X
eurjchem-336	165	5	,	,	PUNCT
eurjchem-336	165	6	51.06	51.06	NUM
eurjchem-336	165	7	;	;	PUNCT
eurjchem-336	165	8	h	h	NOUN
eurjchem-336	165	9	,	,	PUNCT
eurjchem-336	165	10	2.65	2.65	NUM
eurjchem-336	165	11	;	;	PUNCT
eurjchem-336	165	12	n	n	CCONJ
eurjchem-336	165	13	,	,	PUNCT
eurjchem-336	165	14	7.44	7.44	NUM
eurjchem-336	165	15	.	.	PUNCT
eurjchem-336	165	16	found	find	VERB
eurjchem-336	165	17	:	:	PUNCT
eurjchem-336	166	1	c	c	X
eurjchem-336	166	2	,	,	PUNCT
eurjchem-336	166	3	51.15	51.15	NUM
eurjchem-336	166	4	;	;	PUNCT
eurjchem-336	166	5	h	h	NOUN
eurjchem-336	166	6	,	,	PUNCT
eurjchem-336	166	7	2.60	2.60	NUM
eurjchem-336	166	8	;	;	PUNCT
eurjchem-336	166	9	n	n	CCONJ
eurjchem-336	166	10	,	,	PUNCT
eurjchem-336	166	11	7.51	7.51	NUM
eurjchem-336	166	12	%	%	NOUN
eurjchem-336	166	13	.	.	PUNCT
eurjchem-336	167	1	3‐(3‐bromo‐5‐methyl‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐	3‐(3‐bromo‐5‐methyl‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐	NUM
eurjchem-336	167	2	pyrazole‐4‐carbaldehyde	pyrazole‐4‐carbaldehyde	NUM
eurjchem-336	167	3	(	(	PUNCT
eurjchem-336	167	4	3	3	NUM
eurjchem-336	167	5	g	g	NOUN
eurjchem-336	167	6	):	):	PUNCT
eurjchem-336	167	7	yield	yield	NOUN
eurjchem-336	167	8	:	:	PUNCT
eurjchem-336	167	9	85	85	NUM
eurjchem-336	167	10	%	%	NOUN
eurjchem-336	167	11	.	.	PUNCT
eurjchem-336	168	1	m.p	m.p	PROPN
eurjchem-336	168	2	.	.	PROPN
eurjchem-336	168	3	:	:	PUNCT
eurjchem-336	169	1	159‐160	159‐160	NUM
eurjchem-336	169	2	oc	oc	X
eurjchem-336	169	3	.	.	PUNCT
eurjchem-336	169	4	ft‐	ft‐	PROPN
eurjchem-336	169	5	ir	ir	PROPN
eurjchem-336	169	6	(	(	PUNCT
eurjchem-336	169	7	kbr	kbr	PROPN
eurjchem-336	169	8	,	,	PUNCT
eurjchem-336	169	9			PROPN
eurjchem-336	169	10	,	,	PUNCT
eurjchem-336	169	11	cm‐1	cm‐1	PROPN
eurjchem-336	169	12	):	):	PUNCT
eurjchem-336	169	13	3489	3489	NUM
eurjchem-336	169	14	(	(	PUNCT
eurjchem-336	169	15	oh	oh	INTJ
eurjchem-336	169	16	)	)	PUNCT
eurjchem-336	169	17	,	,	PUNCT
eurjchem-336	169	18	1680	1680	NUM
eurjchem-336	169	19	,	,	PUNCT
eurjchem-336	169	20	1645	1645	NUM
eurjchem-336	169	21	.	.	PUNCT
eurjchem-336	170	1	1h	1h	NUM
eurjchem-336	170	2	nmr	nmr	NOUN
eurjchem-336	170	3	(	(	PUNCT
eurjchem-336	170	4	300	300	NUM
eurjchem-336	170	5	mhz	mhz	NOUN
eurjchem-336	170	6	,	,	PUNCT
eurjchem-336	170	7	cdcl3	cdcl3	NOUN
eurjchem-336	170	8	):	):	PUNCT
eurjchem-336	170	9	2.36	2.36	NUM
eurjchem-336	170	10	(	(	PUNCT
eurjchem-336	170	11	s	s	PROPN
eurjchem-336	170	12	,	,	PUNCT
eurjchem-336	170	13	3h	3h	NUM
eurjchem-336	170	14	)	)	PUNCT
eurjchem-336	170	15	,	,	PUNCT
eurjchem-336	170	16	7.44‐7.46	7.44‐7.46	NUM
eurjchem-336	170	17	(	(	PUNCT
eurjchem-336	170	18	m	m	PROPN
eurjchem-336	170	19	,	,	PUNCT
eurjchem-336	170	20	2h	2h	NUM
eurjchem-336	170	21	)	)	PUNCT
eurjchem-336	170	22	,	,	PUNCT
eurjchem-336	170	23	7.54	7.54	NUM
eurjchem-336	170	24	(	(	PUNCT
eurjchem-336	170	25	t	t	PROPN
eurjchem-336	170	26	,	,	PUNCT
eurjchem-336	170	27	2h	2h	NUM
eurjchem-336	170	28	,	,	PUNCT
eurjchem-336	170	29	j	j	PROPN
eurjchem-336	170	30	=	=	SYM
eurjchem-336	170	31	7.2	7.2	NUM
eurjchem-336	170	32	hz	hz	NOUN
eurjchem-336	170	33	)	)	PUNCT
eurjchem-336	170	34	,	,	PUNCT
eurjchem-336	170	35	7.72‐7.75	7.72‐7.75	NUM
eurjchem-336	170	36	(	(	PUNCT
eurjchem-336	170	37	m	m	PROPN
eurjchem-336	170	38	,	,	PUNCT
eurjchem-336	170	39	3h	3h	NUM
eurjchem-336	170	40	)	)	PUNCT
eurjchem-336	170	41	,	,	PUNCT
eurjchem-336	170	42	8.59	8.59	NUM
eurjchem-336	170	43	(	(	PUNCT
eurjchem-336	170	44	s	s	PROPN
eurjchem-336	170	45	,	,	PUNCT
eurjchem-336	170	46	1h	1h	NUM
eurjchem-336	170	47	)	)	PUNCT
eurjchem-336	170	48	,	,	PUNCT
eurjchem-336	170	49	10.17	10.17	NUM
eurjchem-336	170	50	(	(	PUNCT
eurjchem-336	170	51	s	s	PROPN
eurjchem-336	170	52	,	,	PUNCT
eurjchem-336	170	53	1h	1h	NUM
eurjchem-336	170	54	)	)	PUNCT
eurjchem-336	170	55	,	,	PUNCT
eurjchem-336	170	56	10.40	10.40	NUM
eurjchem-336	170	57	(	(	PUNCT
eurjchem-336	170	58	s	s	PROPN
eurjchem-336	170	59	,	,	PUNCT
eurjchem-336	170	60	1h	1h	NUM
eurjchem-336	170	61	)	)	PUNCT
eurjchem-336	170	62	.	.	PUNCT
eurjchem-336	171	1	13c	13c	NOUN
eurjchem-336	171	2	nmr	nmr	NOUN
eurjchem-336	171	3	(	(	PUNCT
eurjchem-336	171	4	75	75	NUM
eurjchem-336	171	5	mhz	mhz	NOUN
eurjchem-336	171	6	,	,	PUNCT
eurjchem-336	171	7	cdcl3	cdcl3	NOUN
eurjchem-336	171	8	):	):	PUNCT
eurjchem-336	171	9	22.8	22.8	NUM
eurjchem-336	171	10	,	,	PUNCT
eurjchem-336	171	11	116.1	116.1	NUM
eurjchem-336	171	12	,	,	PUNCT
eurjchem-336	171	13	115.5	115.5	NUM
eurjchem-336	171	14	,	,	PUNCT
eurjchem-336	171	15	119.3	119.3	NUM
eurjchem-336	171	16	,	,	PUNCT
eurjchem-336	171	17	123.7	123.7	NUM
eurjchem-336	171	18	,	,	PUNCT
eurjchem-336	171	19	128.2	128.2	NUM
eurjchem-336	171	20	,	,	PUNCT
eurjchem-336	171	21	131.4	131.4	NUM
eurjchem-336	171	22	,	,	PUNCT
eurjchem-336	171	23	132.1	132.1	NUM
eurjchem-336	171	24	,	,	PUNCT
eurjchem-336	171	25	133.0	133.0	NUM
eurjchem-336	171	26	,	,	PUNCT
eurjchem-336	171	27	134.7	134.7	NUM
eurjchem-336	171	28	,	,	PUNCT
eurjchem-336	171	29	135.3	135.3	NUM
eurjchem-336	171	30	,	,	PUNCT
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eurjchem-336	171	32	,	,	PUNCT
eurjchem-336	171	33	151.0	151.0	NUM
eurjchem-336	171	34	,	,	PUNCT
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eurjchem-336	171	36	,	,	PUNCT
eurjchem-336	171	37	182.8	182.8	NUM
eurjchem-336	171	38	.	.	PUNCT
eurjchem-336	172	1	ms	ms	NOUN
eurjchem-336	172	2	(	(	PUNCT
eurjchem-336	172	3	ei	ei	PROPN
eurjchem-336	172	4	,	,	PUNCT
eurjchem-336	172	5	m	m	PROPN
eurjchem-336	172	6	/	/	SYM
eurjchem-336	172	7	z	z	NUM
eurjchem-336	172	8	):	):	PUNCT
eurjchem-336	172	9	358	358	NUM
eurjchem-336	172	10	(	(	PUNCT
eurjchem-336	172	11	m+2	m+2	NOUN
eurjchem-336	172	12	)	)	PUNCT
eurjchem-336	172	13	,	,	PUNCT
eurjchem-336	172	14	356	356	NUM
eurjchem-336	172	15	(	(	PUNCT
eurjchem-336	172	16	m+	m+	NUM
eurjchem-336	172	17	)	)	PUNCT
eurjchem-336	172	18	.	.	PUNCT
eurjchem-336	173	1	anal	anal	PROPN
eurjchem-336	173	2	.	.	PUNCT
eurjchem-336	173	3	calcd	calcd	NOUN
eurjchem-336	173	4	.	.	PUNCT
eurjchem-336	174	1	for	for	ADP
eurjchem-336	174	2	c17h13n2o2br	c17h13n2o2br	PROPN
eurjchem-336	174	3	:	:	PUNCT
eurjchem-336	174	4	c	c	X
eurjchem-336	174	5	,	,	PUNCT
eurjchem-336	174	6	57.30	57.30	NUM
eurjchem-336	174	7	;	;	PUNCT
eurjchem-336	174	8	h	h	NOUN
eurjchem-336	174	9	,	,	PUNCT
eurjchem-336	174	10	3.65	3.65	NUM
eurjchem-336	174	11	;	;	PUNCT
eurjchem-336	174	12	n	n	CCONJ
eurjchem-336	174	13	,	,	PUNCT
eurjchem-336	174	14	7.85	7.85	NUM
eurjchem-336	174	15	.	.	PUNCT
eurjchem-336	174	16	found	find	VERB
eurjchem-336	174	17	:	:	PUNCT
eurjchem-336	175	1	c	c	X
eurjchem-336	175	2	,	,	PUNCT
eurjchem-336	175	3	57.49	57.49	NUM
eurjchem-336	175	4	;	;	PUNCT
eurjchem-336	176	1	h	h	NOUN
eurjchem-336	176	2	,	,	PUNCT
eurjchem-336	176	3	3.71	3.71	NUM
eurjchem-336	176	4	;	;	PUNCT
eurjchem-336	176	5	n	n	CCONJ
eurjchem-336	176	6	,	,	PUNCT
eurjchem-336	176	7	7.93	7.93	NUM
eurjchem-336	176	8	%	%	NOUN
eurjchem-336	176	9	.	.	PUNCT
eurjchem-336	177	1	2.2.4	2.2.4	X
eurjchem-336	177	2	.	.	PUNCT
eurjchem-336	177	3	general	general	ADJ
eurjchem-336	177	4	procedure	procedure	NOUN
eurjchem-336	177	5	for	for	ADP
eurjchem-336	177	6	the	the	DET
eurjchem-336	177	7	preparation	preparation	NOUN
eurjchem-336	177	8	of	of	ADP
eurjchem-336	177	9	3‐(2‐	3‐(2‐	PROPN
eurjchem-336	177	10	(	(	PUNCT
eurjchem-336	177	11	allyloxy	allyloxy	ADJ
eurjchem-336	177	12	aryl)‐1‐phenyl‐1h‐pyrazole‐4‐carbaldehyde	aryl)‐1‐phenyl‐1h‐pyrazole‐4‐carbaldehyde	NOUN
eurjchem-336	177	13	(	(	PUNCT
eurjchem-336	177	14	4a‐	4a‐	NUM
eurjchem-336	177	15	g	g	NOUN
eurjchem-336	177	16	)	)	PUNCT
eurjchem-336	177	17	to	to	ADP
eurjchem-336	177	18	a	a	DET
eurjchem-336	177	19	solution	solution	NOUN
eurjchem-336	177	20	of	of	ADP
eurjchem-336	177	21	3‐aryl‐4‐formylpyrazole	3‐aryl‐4‐formylpyrazole	PROPN
eurjchem-336	177	22	(	(	PUNCT
eurjchem-336	177	23	3.5	3.5	NUM
eurjchem-336	177	24	mmol	mmol	NOUN
eurjchem-336	177	25	)	)	PUNCT
eurjchem-336	177	26	in	in	ADP
eurjchem-336	177	27	dmso	dmso	NOUN
eurjchem-336	177	28	(	(	PUNCT
eurjchem-336	177	29	10	10	NUM
eurjchem-336	177	30	ml	ml	NOUN
eurjchem-336	177	31	)	)	PUNCT
eurjchem-336	177	32	,	,	PUNCT
eurjchem-336	177	33	k2co3	k2co3	ADJ
eurjchem-336	177	34	(	(	PUNCT
eurjchem-336	177	35	8	8	NUM
eurjchem-336	177	36	mmol	mmol	NOUN
eurjchem-336	177	37	)	)	PUNCT
eurjchem-336	177	38	and	and	CCONJ
eurjchem-336	177	39	ally	ally	NOUN
eurjchem-336	177	40	bromide	bromide	NOUN
eurjchem-336	177	41	(	(	PUNCT
eurjchem-336	177	42	3.55	3.55	NUM
eurjchem-336	177	43	mmol	mmol	NOUN
eurjchem-336	177	44	)	)	PUNCT
eurjchem-336	177	45	was	be	AUX
eurjchem-336	177	46	added	add	VERB
eurjchem-336	177	47	.	.	PUNCT
eurjchem-336	178	1	the	the	DET
eurjchem-336	178	2	reaction	reaction	NOUN
eurjchem-336	178	3	mixture	mixture	NOUN
eurjchem-336	178	4	was	be	AUX
eurjchem-336	178	5	stirred	stir	VERB
eurjchem-336	178	6	at	at	ADP
eurjchem-336	178	7	room	room	NOUN
eurjchem-336	178	8	temperature	temperature	NOUN
eurjchem-336	178	9	for	for	ADP
eurjchem-336	178	10	4h	4h	NUM
eurjchem-336	178	11	.	.	PUNCT
eurjchem-336	179	1	then	then	ADV
eurjchem-336	179	2	the	the	DET
eurjchem-336	179	3	reaction	reaction	NOUN
eurjchem-336	179	4	mixture	mixture	NOUN
eurjchem-336	179	5	was	be	AUX
eurjchem-336	179	6	poured	pour	VERB
eurjchem-336	179	7	onto	onto	ADP
eurjchem-336	179	8	crushed	crush	VERB
eurjchem-336	179	9	ice	ice	NOUN
eurjchem-336	179	10	.	.	PUNCT
eurjchem-336	180	1	the	the	DET
eurjchem-336	180	2	precipitation	precipitation	NOUN
eurjchem-336	180	3	was	be	AUX
eurjchem-336	180	4	filtered	filter	VERB
eurjchem-336	180	5	and	and	CCONJ
eurjchem-336	180	6	crystallized	crystallize	VERB
eurjchem-336	180	7	by	by	ADP
eurjchem-336	180	8	methanol	methanol	NOUN
eurjchem-336	180	9	.	.	PUNCT
eurjchem-336	181	1	3‐(2‐(allyloxy)‐5‐chlorophenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	3‐(2‐(allyloxy)‐5‐chlorophenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	NUM
eurjchem-336	181	2	carbaldehyde	carbaldehyde	NOUN
eurjchem-336	181	3	(	(	PUNCT
eurjchem-336	181	4	4a	4a	NUM
eurjchem-336	181	5	):	):	PUNCT
eurjchem-336	181	6	yield	yield	NOUN
eurjchem-336	181	7	:	:	PUNCT
eurjchem-336	181	8	87	87	NUM
eurjchem-336	181	9	%	%	NOUN
eurjchem-336	181	10	.	.	PUNCT
eurjchem-336	182	1	m.p	m.p	PROPN
eurjchem-336	182	2	.	.	PROPN
eurjchem-336	182	3	:	:	PUNCT
eurjchem-336	183	1	121‐123	121‐123	NUM
eurjchem-336	183	2	oc	oc	X
eurjchem-336	183	3	.	.	PUNCT
eurjchem-336	183	4	ft‐ir	ft‐ir	NOUN
eurjchem-336	183	5	(	(	PUNCT
eurjchem-336	183	6	kbr	kbr	PROPN
eurjchem-336	183	7	,	,	PUNCT
eurjchem-336	183	8			PROPN
eurjchem-336	183	9	,	,	PUNCT
eurjchem-336	183	10	cm‐1	cm‐1	PROPN
eurjchem-336	183	11	):	):	PUNCT
eurjchem-336	183	12	1672	1672	NUM
eurjchem-336	183	13	,	,	PUNCT
eurjchem-336	183	14	1650	1650	NUM
eurjchem-336	183	15	.	.	PUNCT
eurjchem-336	184	1	1h	1h	NUM
eurjchem-336	184	2	nmr	nmr	NOUN
eurjchem-336	184	3	(	(	PUNCT
eurjchem-336	184	4	300	300	NUM
eurjchem-336	184	5	mhz	mhz	NOUN
eurjchem-336	184	6	,	,	PUNCT
eurjchem-336	184	7	cdcl3	cdcl3	NOUN
eurjchem-336	184	8	):	):	PUNCT
eurjchem-336	184	9	4.55	4.55	NUM
eurjchem-336	184	10	(	(	PUNCT
eurjchem-336	184	11	d	d	PROPN
eurjchem-336	184	12	,	,	PUNCT
eurjchem-336	184	13	2h	2h	NUM
eurjchem-336	184	14	,	,	PUNCT
eurjchem-336	184	15	j	j	PROPN
eurjchem-336	184	16	=	=	SYM
eurjchem-336	184	17	5.1	5.1	NUM
eurjchem-336	184	18	hz	hz	NOUN
eurjchem-336	184	19	)	)	PUNCT
eurjchem-336	184	20	,	,	PUNCT
eurjchem-336	184	21	5.24	5.24	NUM
eurjchem-336	184	22	(	(	PUNCT
eurjchem-336	184	23	d	d	PROPN
eurjchem-336	184	24	,	,	PUNCT
eurjchem-336	184	25	1h	1h	NUM
eurjchem-336	184	26	,	,	PUNCT
eurjchem-336	184	27	j	j	PROPN
eurjchem-336	184	28	=	=	PROPN
eurjchem-336	184	29	10.8	10.8	NUM
eurjchem-336	184	30	hz	hz	NOUN
eurjchem-336	184	31	)	)	PUNCT
eurjchem-336	184	32	,	,	PUNCT
eurjchem-336	184	33	5.31	5.31	NUM
eurjchem-336	184	34	(	(	PUNCT
eurjchem-336	184	35	d	d	PROPN
eurjchem-336	184	36	,	,	PUNCT
eurjchem-336	184	37	1h	1h	NUM
eurjchem-336	184	38	,	,	PUNCT
eurjchem-336	184	39	j	j	PROPN
eurjchem-336	185	1	=	=	PROPN
eurjchem-336	185	2	17.1	17.1	NUM
eurjchem-336	185	3	hz	hz	NOUN
eurjchem-336	185	4	)	)	PUNCT
eurjchem-336	185	5	,	,	PUNCT
eurjchem-336	185	6	5.93	5.93	NUM
eurjchem-336	185	7	(	(	PUNCT
eurjchem-336	185	8	m	m	PROPN
eurjchem-336	185	9	,	,	PUNCT
eurjchem-336	185	10	1h	1h	NUM
eurjchem-336	185	11	)	)	PUNCT
eurjchem-336	185	12	,	,	PUNCT
eurjchem-336	185	13	6.95	6.95	NUM
eurjchem-336	185	14	(	(	PUNCT
eurjchem-336	185	15	d	d	PROPN
eurjchem-336	185	16	,	,	PUNCT
eurjchem-336	185	17	1h	1h	NUM
eurjchem-336	185	18	,	,	PUNCT
eurjchem-336	185	19	j	j	PROPN
eurjchem-336	185	20	=	=	PROPN
eurjchem-336	185	21	8.7	8.7	NUM
eurjchem-336	185	22	hz	hz	NOUN
eurjchem-336	185	23	)	)	PUNCT
eurjchem-336	185	24	,	,	PUNCT
eurjchem-336	185	25	7.36‐7.41	7.36‐7.41	PROPN
eurjchem-336	185	26	(	(	PUNCT
eurjchem-336	185	27	m	m	PROPN
eurjchem-336	185	28	,	,	PUNCT
eurjchem-336	185	29	2h	2h	NUM
eurjchem-336	185	30	)	)	PUNCT
eurjchem-336	185	31	,	,	PUNCT
eurjchem-336	185	32	7.51	7.51	NUM
eurjchem-336	185	33	(	(	PUNCT
eurjchem-336	185	34	t	t	PROPN
eurjchem-336	185	35	,	,	PUNCT
eurjchem-336	185	36	2h	2h	NUM
eurjchem-336	185	37	,	,	PUNCT
eurjchem-336	185	38	j	j	PROPN
eurjchem-336	185	39	=	=	PROPN
eurjchem-336	185	40	8.4	8.4	NUM
eurjchem-336	185	41	hz	hz	NOUN
eurjchem-336	185	42	)	)	PUNCT
eurjchem-336	185	43	,	,	PUNCT
eurjchem-336	185	44	7.62	7.62	NUM
eurjchem-336	185	45	(	(	PUNCT
eurjchem-336	185	46	d	d	PROPN
eurjchem-336	185	47	,	,	PUNCT
eurjchem-336	185	48	1h	1h	NUM
eurjchem-336	185	49	,	,	PUNCT
eurjchem-336	185	50	j	j	PROPN
eurjchem-336	185	51	=	=	SYM
eurjchem-336	185	52	2.4	2.4	NUM
eurjchem-336	185	53	hz	hz	NOUN
eurjchem-336	185	54	)	)	PUNCT
eurjchem-336	185	55	,	,	PUNCT
eurjchem-336	185	56	7.77	7.77	NUM
eurjchem-336	185	57	(	(	PUNCT
eurjchem-336	185	58	d	d	PROPN
eurjchem-336	185	59	,	,	PUNCT
eurjchem-336	185	60	2h	2h	NUM
eurjchem-336	185	61	,	,	PUNCT
eurjchem-336	185	62	j	j	PROPN
eurjchem-336	185	63	=	=	PROPN
eurjchem-336	185	64	8.7	8.7	NUM
eurjchem-336	185	65	hz	hz	NOUN
eurjchem-336	185	66	)	)	PUNCT
eurjchem-336	185	67	,	,	PUNCT
eurjchem-336	185	68	8.51	8.51	NUM
eurjchem-336	185	69	(	(	PUNCT
eurjchem-336	185	70	s	s	PROPN
eurjchem-336	185	71	,	,	PUNCT
eurjchem-336	185	72	1h	1h	NUM
eurjchem-336	185	73	)	)	PUNCT
eurjchem-336	185	74	,	,	PUNCT
eurjchem-336	185	75	9.82	9.82	NUM
eurjchem-336	185	76	(	(	PUNCT
eurjchem-336	185	77	s	s	PROPN
eurjchem-336	185	78	,	,	PUNCT
eurjchem-336	185	79	1h	1h	NUM
eurjchem-336	185	80	)	)	PUNCT
eurjchem-336	185	81	.	.	PUNCT
eurjchem-336	186	1	13c	13c	NOUN
eurjchem-336	186	2	nmr	nmr	NOUN
eurjchem-336	186	3	(	(	PUNCT
eurjchem-336	186	4	75	75	NUM
eurjchem-336	186	5	mhz	mhz	NOUN
eurjchem-336	186	6	,	,	PUNCT
eurjchem-336	186	7	cdcl3	cdcl3	NOUN
eurjchem-336	186	8	):	):	PUNCT
eurjchem-336	186	9	69.5	69.5	NUM
eurjchem-336	186	10	,	,	PUNCT
eurjchem-336	186	11	113.7	113.7	NUM
eurjchem-336	186	12	,	,	PUNCT
eurjchem-336	186	13	118.0	118.0	NUM
eurjchem-336	186	14	,	,	PUNCT
eurjchem-336	186	15	119.4	119.4	NUM
eurjchem-336	186	16	,	,	PUNCT
eurjchem-336	186	17	122.3	122.3	NUM
eurjchem-336	186	18	,	,	PUNCT
eurjchem-336	186	19	123.2	123.2	NUM
eurjchem-336	186	20	,	,	PUNCT
eurjchem-336	186	21	126.1	126.1	NUM
eurjchem-336	186	22	,	,	PUNCT
eurjchem-336	186	23	127.7	127.7	NUM
eurjchem-336	186	24	,	,	PUNCT
eurjchem-336	186	25	129.1	129.1	NUM
eurjchem-336	186	26	,	,	PUNCT
eurjchem-336	186	27	129.5	129.5	NUM
eurjchem-336	186	28	,	,	PUNCT
eurjchem-336	186	29	130.2	130.2	NUM
eurjchem-336	186	30	,	,	PUNCT
eurjchem-336	186	31	130.9	130.9	NUM
eurjchem-336	186	32	,	,	PUNCT
eurjchem-336	186	33	132.0	132.0	NUM
eurjchem-336	186	34	,	,	PUNCT
eurjchem-336	186	35	138.9	138.9	NUM
eurjchem-336	186	36	,	,	PUNCT
eurjchem-336	186	37	150.4	150.4	NUM
eurjchem-336	186	38	,	,	PUNCT
eurjchem-336	186	39	154.5	154.5	NUM
eurjchem-336	186	40	,	,	PUNCT
eurjchem-336	186	41	185.9	185.9	NUM
eurjchem-336	186	42	.	.	PUNCT
eurjchem-336	187	1	ms	ms	PROPN
eurjchem-336	187	2	(	(	PUNCT
eurjchem-336	187	3	ei	ei	PROPN
eurjchem-336	187	4	,	,	PUNCT
eurjchem-336	187	5	m	m	PROPN
eurjchem-336	187	6	/	/	SYM
eurjchem-336	187	7	z	z	NOUN
eurjchem-336	187	8	):	):	PUNCT
eurjchem-336	187	9	338	338	NUM
eurjchem-336	187	10	(	(	PUNCT
eurjchem-336	187	11	m+	m+	NUM
eurjchem-336	187	12	)	)	PUNCT
eurjchem-336	187	13	.	.	PUNCT
eurjchem-336	188	1	anal	anal	PROPN
eurjchem-336	188	2	.	.	PUNCT
eurjchem-336	188	3	calcd	calcd	NOUN
eurjchem-336	188	4	.	.	PUNCT
eurjchem-336	189	1	for	for	ADP
eurjchem-336	189	2	c19h15n2o2cl	c19h15n2o2cl	NOUN
eurjchem-336	189	3	:	:	PUNCT
eurjchem-336	189	4	c	c	X
eurjchem-336	189	5	,	,	PUNCT
eurjchem-336	189	6	67.45	67.45	NUM
eurjchem-336	189	7	;	;	PUNCT
eurjchem-336	189	8	h	h	NOUN
eurjchem-336	189	9	,	,	PUNCT
eurjchem-336	189	10	4.43	4.43	NUM
eurjchem-336	189	11	;	;	PUNCT
eurjchem-336	189	12	n	n	CCONJ
eurjchem-336	189	13	,	,	PUNCT
eurjchem-336	189	14	8.28	8.28	NUM
eurjchem-336	189	15	.	.	PUNCT
eurjchem-336	189	16	found	find	VERB
eurjchem-336	189	17	:	:	PUNCT
eurjchem-336	190	1	c	c	X
eurjchem-336	190	2	,	,	PUNCT
eurjchem-336	190	3	67.58	67.58	NUM
eurjchem-336	190	4	;	;	PUNCT
eurjchem-336	190	5	h	h	NOUN
eurjchem-336	190	6	,	,	PUNCT
eurjchem-336	190	7	4.31	4.31	NUM
eurjchem-336	190	8	;	;	PUNCT
eurjchem-336	190	9	n	n	CCONJ
eurjchem-336	190	10	,	,	PUNCT
eurjchem-336	190	11	8.35	8.35	NUM
eurjchem-336	190	12	%	%	NOUN
eurjchem-336	190	13	.	.	PUNCT
eurjchem-336	191	1	3‐(2‐(allyloxy)‐5‐bromophenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	3‐(2‐(allyloxy)‐5‐bromophenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	NUM
eurjchem-336	191	2	carbaldehyde	carbaldehyde	NOUN
eurjchem-336	191	3	(	(	PUNCT
eurjchem-336	191	4	4b	4b	X
eurjchem-336	191	5	):	):	PUNCT
eurjchem-336	191	6	yield	yield	NOUN
eurjchem-336	191	7	:	:	PUNCT
eurjchem-336	191	8	89	89	NUM
eurjchem-336	191	9	%	%	NOUN
eurjchem-336	191	10	.	.	PUNCT
eurjchem-336	192	1	m.p	m.p	PROPN
eurjchem-336	192	2	.	.	PROPN
eurjchem-336	192	3	:	:	PUNCT
eurjchem-336	193	1	128‐129	128‐129	PROPN
eurjchem-336	193	2	oc	oc	NOUN
eurjchem-336	193	3	.	.	PUNCT
eurjchem-336	193	4	ft‐ir	ft‐ir	NOUN
eurjchem-336	193	5	(	(	PUNCT
eurjchem-336	193	6	kbr	kbr	PROPN
eurjchem-336	193	7	,	,	PUNCT
eurjchem-336	193	8			PROPN
eurjchem-336	193	9	,	,	PUNCT
eurjchem-336	193	10	cm‐1	cm‐1	PROPN
eurjchem-336	193	11	):	):	PUNCT
eurjchem-336	193	12	1675	1675	NUM
eurjchem-336	193	13	,	,	PUNCT
eurjchem-336	193	14	1658	1658	NUM
eurjchem-336	193	15	.	.	PUNCT
eurjchem-336	194	1	1h	1h	NUM
eurjchem-336	194	2	nmr	nmr	NOUN
eurjchem-336	194	3	(	(	PUNCT
eurjchem-336	194	4	300	300	NUM
eurjchem-336	194	5	mhz	mhz	NOUN
eurjchem-336	194	6	,	,	PUNCT
eurjchem-336	194	7	cdcl3	cdcl3	NOUN
eurjchem-336	194	8	):	):	PUNCT
eurjchem-336	194	9	4.58	4.58	NUM
eurjchem-336	194	10	(	(	PUNCT
eurjchem-336	194	11	d	d	NOUN
eurjchem-336	194	12	,	,	PUNCT
eurjchem-336	194	13	2h	2h	NUM
eurjchem-336	194	14	,	,	PUNCT
eurjchem-336	194	15	j	j	PROPN
eurjchem-336	194	16	=	=	PROPN
eurjchem-336	194	17	5.4	5.4	NUM
eurjchem-336	194	18	hz	hz	NOUN
eurjchem-336	194	19	)	)	PUNCT
eurjchem-336	194	20	,	,	PUNCT
eurjchem-336	194	21	5.21	5.21	NUM
eurjchem-336	194	22	(	(	PUNCT
eurjchem-336	194	23	d	d	PROPN
eurjchem-336	194	24	,	,	PUNCT
eurjchem-336	194	25	1h	1h	NUM
eurjchem-336	194	26	,	,	PUNCT
eurjchem-336	194	27	j	j	PROPN
eurjchem-336	194	28	=	=	PROPN
eurjchem-336	194	29	10.5	10.5	NUM
eurjchem-336	194	30	hz	hz	NOUN
eurjchem-336	194	31	)	)	PUNCT
eurjchem-336	194	32	,	,	PUNCT
eurjchem-336	194	33	5.40	5.40	NUM
eurjchem-336	194	34	(	(	PUNCT
eurjchem-336	194	35	d	d	PROPN
eurjchem-336	194	36	,	,	PUNCT
eurjchem-336	194	37	1h	1h	NUM
eurjchem-336	194	38	,	,	PUNCT
eurjchem-336	194	39	j	j	PROPN
eurjchem-336	194	40	=	=	PROPN
eurjchem-336	194	41	17.4	17.4	NUM
eurjchem-336	194	42	hz	hz	NOUN
eurjchem-336	194	43	)	)	PUNCT
eurjchem-336	194	44	,	,	PUNCT
eurjchem-336	194	45	5.91	5.91	NUM
eurjchem-336	194	46	(	(	PUNCT
eurjchem-336	194	47	m	m	PROPN
eurjchem-336	194	48	,	,	PUNCT
eurjchem-336	194	49	1h	1h	NUM
eurjchem-336	194	50	)	)	PUNCT
eurjchem-336	194	51	,	,	PUNCT
eurjchem-336	194	52	6.88	6.88	NUM
eurjchem-336	194	53	(	(	PUNCT
eurjchem-336	194	54	d	d	PROPN
eurjchem-336	194	55	,	,	PUNCT
eurjchem-336	194	56	1h	1h	NUM
eurjchem-336	194	57	,	,	PUNCT
eurjchem-336	194	58	j	j	PROPN
eurjchem-336	194	59	=	=	PROPN
eurjchem-336	194	60	8.7	8.7	NUM
eurjchem-336	194	61	hz	hz	NOUN
eurjchem-336	194	62	)	)	PUNCT
eurjchem-336	194	63	,	,	PUNCT
eurjchem-336	194	64	7.32‐7.41	7.32‐7.41	NUM
eurjchem-336	194	65	(	(	PUNCT
eurjchem-336	194	66	m	m	PROPN
eurjchem-336	194	67	,	,	PUNCT
eurjchem-336	194	68	2h	2h	NUM
eurjchem-336	194	69	)	)	PUNCT
eurjchem-336	194	70	,	,	PUNCT
eurjchem-336	194	71	7.50	7.50	NUM
eurjchem-336	194	72	(	(	PUNCT
eurjchem-336	194	73	t	t	PROPN
eurjchem-336	194	74	,	,	PUNCT
eurjchem-336	194	75	2h	2h	NUM
eurjchem-336	194	76	,	,	PUNCT
eurjchem-336	194	77	j	j	PROPN
eurjchem-336	194	78	=	=	PROPN
eurjchem-336	194	79	8.4	8.4	NUM
eurjchem-336	194	80	hz	hz	NOUN
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eurjchem-336	194	82	,	,	PUNCT
eurjchem-336	194	83	7.74	7.74	NUM
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eurjchem-336	194	85	d	d	PROPN
eurjchem-336	194	86	,	,	PUNCT
eurjchem-336	194	87	1h	1h	NUM
eurjchem-336	194	88	,	,	PUNCT
eurjchem-336	194	89	j	j	PROPN
eurjchem-336	194	90	=	=	SYM
eurjchem-336	194	91	2.4	2.4	NUM
eurjchem-336	194	92	hz	hz	NOUN
eurjchem-336	194	93	)	)	PUNCT
eurjchem-336	194	94	,	,	PUNCT
eurjchem-336	194	95	7.86	7.86	NUM
eurjchem-336	194	96	(	(	PUNCT
eurjchem-336	194	97	d	d	NOUN
eurjchem-336	194	98	,	,	PUNCT
eurjchem-336	194	99	2h	2h	NUM
eurjchem-336	194	100	,	,	PUNCT
eurjchem-336	194	101	j	j	PROPN
eurjchem-336	194	102	=	=	PROPN
eurjchem-336	194	103	8.4	8.4	NUM
eurjchem-336	194	104	hz	hz	NOUN
eurjchem-336	194	105	)	)	PUNCT
eurjchem-336	194	106	,	,	PUNCT
eurjchem-336	194	107	8.53	8.53	NUM
eurjchem-336	194	108	(	(	PUNCT
eurjchem-336	194	109	s	s	PROPN
eurjchem-336	194	110	,	,	PUNCT
eurjchem-336	194	111	1h	1h	NUM
eurjchem-336	194	112	)	)	PUNCT
eurjchem-336	194	113	,	,	PUNCT
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eurjchem-336	194	116	s	s	PROPN
eurjchem-336	194	117	,	,	PUNCT
eurjchem-336	194	118	1h	1h	NUM
eurjchem-336	194	119	)	)	PUNCT
eurjchem-336	194	120	.	.	PUNCT
eurjchem-336	195	1	13c	13c	NOUN
eurjchem-336	195	2	nmr	nmr	NOUN
eurjchem-336	195	3	(	(	PUNCT
eurjchem-336	195	4	75	75	NUM
eurjchem-336	195	5	mhz	mhz	NOUN
eurjchem-336	195	6	,	,	PUNCT
eurjchem-336	195	7	cdcl3	cdcl3	NOUN
eurjchem-336	195	8	):	):	PUNCT
eurjchem-336	195	9	70.1	70.1	NUM
eurjchem-336	195	10	,	,	PUNCT
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eurjchem-336	195	14	,	,	PUNCT
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eurjchem-336	195	18	,	,	PUNCT
eurjchem-336	195	19	122.1	122.1	NUM
eurjchem-336	195	20	,	,	PUNCT
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eurjchem-336	195	22	,	,	PUNCT
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eurjchem-336	195	24	,	,	PUNCT
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eurjchem-336	195	26	,	,	PUNCT
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eurjchem-336	195	28	,	,	PUNCT
eurjchem-336	195	29	132.0	132.0	NUM
eurjchem-336	195	30	,	,	PUNCT
eurjchem-336	195	31	135.7	135.7	NUM
eurjchem-336	195	32	,	,	PUNCT
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eurjchem-336	195	34	,	,	PUNCT
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eurjchem-336	195	38	,	,	PUNCT
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eurjchem-336	195	40	,	,	PUNCT
eurjchem-336	195	41	186.4	186.4	NUM
eurjchem-336	195	42	.	.	PUNCT
eurjchem-336	196	1	ms	ms	PROPN
eurjchem-336	196	2	(	(	PUNCT
eurjchem-336	196	3	ei	ei	PROPN
eurjchem-336	196	4	,	,	PUNCT
eurjchem-336	196	5	m	m	PROPN
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eurjchem-336	196	7	z	z	NOUN
eurjchem-336	196	8	):	):	PUNCT
eurjchem-336	196	9	384	384	NUM
eurjchem-336	196	10	(	(	PUNCT
eurjchem-336	196	11	m+2	m+2	NOUN
eurjchem-336	196	12	)	)	PUNCT
eurjchem-336	196	13	,	,	PUNCT
eurjchem-336	196	14	382	382	NUM
eurjchem-336	196	15	(	(	PUNCT
eurjchem-336	196	16	m+	m+	NUM
eurjchem-336	196	17	)	)	PUNCT
eurjchem-336	196	18	;	;	PUNCT
eurjchem-336	196	19	anal	anal	ADJ
eurjchem-336	196	20	.	.	PUNCT
eurjchem-336	196	21	calcd	calcd	NOUN
eurjchem-336	196	22	.	.	PUNCT
eurjchem-336	197	1	for	for	SCONJ
eurjchem-336	197	2	c19h15n2o2br	c19h15n2o2br	PROPN
eurjchem-336	197	3	:	:	PUNCT
eurjchem-336	197	4	c	c	X
eurjchem-336	197	5	,	,	PUNCT
eurjchem-336	197	6	59.68	59.68	NUM
eurjchem-336	197	7	;	;	PUNCT
eurjchem-336	197	8	h	h	NOUN
eurjchem-336	197	9	,	,	PUNCT
eurjchem-336	197	10	3.92	3.92	NUM
eurjchem-336	197	11	;	;	PUNCT
eurjchem-336	197	12	n	n	CCONJ
eurjchem-336	197	13	,	,	PUNCT
eurjchem-336	197	14	7.32	7.32	NUM
eurjchem-336	197	15	.	.	PUNCT
eurjchem-336	197	16	found	find	VERB
eurjchem-336	197	17	:	:	PUNCT
eurjchem-336	198	1	c	c	X
eurjchem-336	198	2	,	,	PUNCT
eurjchem-336	198	3	60.08	60.08	NUM
eurjchem-336	198	4	;	;	PUNCT
eurjchem-336	198	5	h	h	NOUN
eurjchem-336	198	6	,	,	PUNCT
eurjchem-336	198	7	4.09	4.09	NUM
eurjchem-336	198	8	;	;	PUNCT
eurjchem-336	198	9	n	n	CCONJ
eurjchem-336	198	10	,	,	PUNCT
eurjchem-336	198	11	7.18	7.18	NUM
eurjchem-336	198	12	%	%	NOUN
eurjchem-336	198	13	.	.	PUNCT
eurjchem-336	199	1	3‐(2‐(allyloxy)‐3‐chlorophenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	3‐(2‐(allyloxy)‐3‐chlorophenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	NUM
eurjchem-336	199	2	carbaldehyde	carbaldehyde	NOUN
eurjchem-336	199	3	(	(	PUNCT
eurjchem-336	199	4	4c	4c	NOUN
eurjchem-336	199	5	):	):	PUNCT
eurjchem-336	199	6	yield	yield	NOUN
eurjchem-336	199	7	:	:	PUNCT
eurjchem-336	199	8	88	88	NUM
eurjchem-336	199	9	%	%	NOUN
eurjchem-336	199	10	.	.	PUNCT
eurjchem-336	200	1	m.p	m.p	PROPN
eurjchem-336	200	2	.	.	PROPN
eurjchem-336	200	3	:	:	PUNCT
eurjchem-336	200	4	92‐94	92‐94	NUM
eurjchem-336	200	5	oc	oc	NOUN
eurjchem-336	200	6	.	.	PUNCT
eurjchem-336	201	1	ft‐ir	ft‐ir	NOUN
eurjchem-336	201	2	(	(	PUNCT
eurjchem-336	201	3	kbr	kbr	PROPN
eurjchem-336	201	4	,	,	PUNCT
eurjchem-336	201	5			PROPN
eurjchem-336	201	6	,	,	PUNCT
eurjchem-336	201	7	cm‐	cm‐	NOUN
eurjchem-336	201	8	1	1	NUM
eurjchem-336	201	9	):	):	PUNCT
eurjchem-336	201	10	1678	1678	NUM
eurjchem-336	201	11	,	,	PUNCT
eurjchem-336	201	12	1635	1635	NUM
eurjchem-336	201	13	.	.	PUNCT
eurjchem-336	202	1	1h	1h	NUM
eurjchem-336	202	2	nmr	nmr	NOUN
eurjchem-336	202	3	(	(	PUNCT
eurjchem-336	202	4	300	300	NUM
eurjchem-336	202	5	mhz	mhz	NOUN
eurjchem-336	202	6	,	,	PUNCT
eurjchem-336	202	7	cdcl3	cdcl3	NOUN
eurjchem-336	202	8	):	):	PUNCT
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eurjchem-336	202	10	(	(	PUNCT
eurjchem-336	202	11	d	d	PROPN
eurjchem-336	202	12	,	,	PUNCT
eurjchem-336	202	13	2h	2h	NUM
eurjchem-336	202	14	,	,	PUNCT
eurjchem-336	202	15	j	j	PROPN
eurjchem-336	202	16	=	=	PROPN
eurjchem-336	202	17	6	6	NUM
eurjchem-336	202	18	hz	hz	NOUN
eurjchem-336	202	19	)	)	PUNCT
eurjchem-336	202	20	,	,	PUNCT
eurjchem-336	202	21	5.01	5.01	NUM
eurjchem-336	202	22	(	(	PUNCT
eurjchem-336	202	23	d	d	PROPN
eurjchem-336	202	24	,	,	PUNCT
eurjchem-336	202	25	1h	1h	NUM
eurjchem-336	202	26	,	,	PUNCT
eurjchem-336	202	27	j	j	PROPN
eurjchem-336	202	28	=	=	PROPN
eurjchem-336	202	29	10.5	10.5	NUM
eurjchem-336	202	30	hz	hz	NOUN
eurjchem-336	202	31	)	)	PUNCT
eurjchem-336	202	32	,	,	PUNCT
eurjchem-336	202	33	5.19	5.19	NUM
eurjchem-336	202	34	(	(	PUNCT
eurjchem-336	202	35	d	d	PROPN
eurjchem-336	202	36	,	,	PUNCT
eurjchem-336	202	37	1h	1h	NUM
eurjchem-336	202	38	,	,	PUNCT
eurjchem-336	202	39	j	j	PROPN
eurjchem-336	202	40	=	=	PROPN
eurjchem-336	202	41	16.8	16.8	NUM
eurjchem-336	202	42	hz	hz	NOUN
eurjchem-336	202	43	)	)	PUNCT
eurjchem-336	202	44	,	,	PUNCT
eurjchem-336	202	45	5.82	5.82	NUM
eurjchem-336	202	46	(	(	PUNCT
eurjchem-336	202	47	m	m	PROPN
eurjchem-336	202	48	,	,	PUNCT
eurjchem-336	202	49	1h	1h	NUM
eurjchem-336	202	50	)	)	PUNCT
eurjchem-336	202	51	,	,	PUNCT
eurjchem-336	202	52	7.21	7.21	NUM
eurjchem-336	202	53	(	(	PUNCT
eurjchem-336	202	54	t	t	PROPN
eurjchem-336	202	55	,	,	PUNCT
eurjchem-336	202	56	1h	1h	NUM
eurjchem-336	202	57	,	,	PUNCT
eurjchem-336	202	58	j	j	PROPN
eurjchem-336	202	59	=	=	SYM
eurjchem-336	202	60	7.8	7.8	NUM
eurjchem-336	202	61	hz	hz	NOUN
eurjchem-336	202	62	)	)	PUNCT
eurjchem-336	202	63	,	,	PUNCT
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eurjchem-336	202	66	t	t	PROPN
eurjchem-336	202	67	,	,	PUNCT
eurjchem-336	202	68	1h	1h	NUM
eurjchem-336	202	69	,	,	PUNCT
eurjchem-336	202	70	j	j	PROPN
eurjchem-336	202	71	=	=	SYM
eurjchem-336	202	72	7.5	7.5	NUM
eurjchem-336	202	73	hz	hz	NOUN
eurjchem-336	202	74	)	)	PUNCT
eurjchem-336	202	75	,	,	PUNCT
eurjchem-336	202	76	7.50‐7.57	7.50‐7.57	NUM
eurjchem-336	202	77	(	(	PUNCT
eurjchem-336	202	78	m	m	PROPN
eurjchem-336	202	79	,	,	PUNCT
eurjchem-336	202	80	4h	4h	NOUN
eurjchem-336	202	81	)	)	PUNCT
eurjchem-336	202	82	,	,	PUNCT
eurjchem-336	202	83	7.79	7.79	NUM
eurjchem-336	202	84	(	(	PUNCT
eurjchem-336	202	85	d	d	PROPN
eurjchem-336	202	86	,	,	PUNCT
eurjchem-336	202	87	2h	2h	NUM
eurjchem-336	202	88	,	,	PUNCT
eurjchem-336	202	89	j	j	PROPN
eurjchem-336	202	90	=	=	SYM
eurjchem-336	202	91	7.5	7.5	NUM
eurjchem-336	202	92	hz	hz	NOUN
eurjchem-336	202	93	)	)	PUNCT
eurjchem-336	202	94	,	,	PUNCT
eurjchem-336	202	95	8.54	8.54	NUM
eurjchem-336	202	96	(	(	PUNCT
eurjchem-336	202	97	s	s	PROPN
eurjchem-336	202	98	,	,	PUNCT
eurjchem-336	202	99	1h	1h	NUM
eurjchem-336	202	100	)	)	PUNCT
eurjchem-336	202	101	,	,	PUNCT
eurjchem-336	202	102	9.85	9.85	NUM
eurjchem-336	202	103	(	(	PUNCT
eurjchem-336	202	104	s	s	PROPN
eurjchem-336	202	105	,	,	PUNCT
eurjchem-336	202	106	1h	1h	NUM
eurjchem-336	202	107	)	)	PUNCT
eurjchem-336	202	108	.	.	PUNCT
eurjchem-336	203	1	13c	13c	NOUN
eurjchem-336	203	2	nmr	nmr	NOUN
eurjchem-336	203	3	(	(	PUNCT
eurjchem-336	203	4	75	75	NUM
eurjchem-336	203	5	mhz	mhz	NOUN
eurjchem-336	203	6	,	,	PUNCT
eurjchem-336	203	7	cdcl3	cdcl3	NOUN
eurjchem-336	203	8	):	):	PUNCT
eurjchem-336	203	9	68.4	68.4	NUM
eurjchem-336	203	10	,	,	PUNCT
eurjchem-336	203	11	114.3	114.3	NUM
eurjchem-336	203	12	,	,	PUNCT
eurjchem-336	203	13	119.1	119.1	NUM
eurjchem-336	203	14	,	,	PUNCT
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eurjchem-336	203	16	,	,	PUNCT
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eurjchem-336	203	18	,	,	PUNCT
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eurjchem-336	203	20	,	,	PUNCT
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eurjchem-336	203	22	,	,	PUNCT
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eurjchem-336	203	24	,	,	PUNCT
eurjchem-336	203	25	129.5	129.5	NUM
eurjchem-336	203	26	,	,	PUNCT
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eurjchem-336	203	28	,	,	PUNCT
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eurjchem-336	203	30	,	,	PUNCT
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eurjchem-336	203	32	,	,	PUNCT
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eurjchem-336	203	34	,	,	PUNCT
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eurjchem-336	203	36	,	,	PUNCT
eurjchem-336	203	37	151.6	151.6	NUM
eurjchem-336	203	38	,	,	PUNCT
eurjchem-336	203	39	155.5	155.5	NUM
eurjchem-336	203	40	,	,	PUNCT
eurjchem-336	203	41	186.8	186.8	NUM
eurjchem-336	203	42	.	.	PUNCT
eurjchem-336	204	1	ms	ms	PROPN
eurjchem-336	204	2	(	(	PUNCT
eurjchem-336	204	3	ei	ei	PROPN
eurjchem-336	204	4	,	,	PUNCT
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eurjchem-336	204	7	z	z	NOUN
eurjchem-336	204	8	):	):	PUNCT
eurjchem-336	204	9	338	338	NUM
eurjchem-336	204	10	(	(	PUNCT
eurjchem-336	204	11	m+	m+	NUM
eurjchem-336	204	12	)	)	PUNCT
eurjchem-336	204	13	.	.	PUNCT
eurjchem-336	205	1	anal	anal	PROPN
eurjchem-336	205	2	.	.	PUNCT
eurjchem-336	205	3	calcd	calcd	NOUN
eurjchem-336	205	4	.	.	PUNCT
eurjchem-336	206	1	for	for	ADP
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eurjchem-336	206	3	:	:	PUNCT
eurjchem-336	206	4	c	c	X
eurjchem-336	206	5	,	,	PUNCT
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eurjchem-336	206	7	;	;	PUNCT
eurjchem-336	206	8	h	h	NOUN
eurjchem-336	206	9	,	,	PUNCT
eurjchem-336	206	10	4.43	4.43	NUM
eurjchem-336	206	11	;	;	PUNCT
eurjchem-336	206	12	n	n	CCONJ
eurjchem-336	206	13	,	,	PUNCT
eurjchem-336	206	14	8.28	8.28	NUM
eurjchem-336	206	15	.	.	PUNCT
eurjchem-336	206	16	found	find	VERB
eurjchem-336	206	17	:	:	PUNCT
eurjchem-336	207	1	c	c	X
eurjchem-336	207	2	,	,	PUNCT
eurjchem-336	207	3	67.15	67.15	NUM
eurjchem-336	207	4	;	;	PUNCT
eurjchem-336	208	1	h	h	NOUN
eurjchem-336	208	2	,	,	PUNCT
eurjchem-336	208	3	4.39	4.39	NUM
eurjchem-336	208	4	;	;	PUNCT
eurjchem-336	208	5	n	n	CCONJ
eurjchem-336	208	6	,	,	PUNCT
eurjchem-336	208	7	8.31	8.31	NUM
eurjchem-336	208	8	%	%	NOUN
eurjchem-336	208	9	.	.	PUNCT
eurjchem-336	209	1	3‐(2‐(allyloxy)‐5,3‐dichlorophenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	3‐(2‐(allyloxy)‐5,3‐dichlorophenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	NUM
eurjchem-336	209	2	carbaldehyde	carbaldehyde	NOUN
eurjchem-336	209	3	(	(	PUNCT
eurjchem-336	209	4	4d	4d	NUM
eurjchem-336	209	5	):	):	PUNCT
eurjchem-336	209	6	yield	yield	NOUN
eurjchem-336	209	7	:	:	PUNCT
eurjchem-336	209	8	90	90	NUM
eurjchem-336	209	9	%	%	NOUN
eurjchem-336	209	10	.	.	PUNCT
eurjchem-336	210	1	m.p	m.p	PROPN
eurjchem-336	210	2	.	.	PROPN
eurjchem-336	210	3	:	:	PUNCT
eurjchem-336	211	1	114‐116	114‐116	NUM
eurjchem-336	211	2	oc	oc	PROPN
eurjchem-336	211	3	.	.	PUNCT
eurjchem-336	211	4	ft‐ir	ft‐ir	NOUN
eurjchem-336	211	5	(	(	PUNCT
eurjchem-336	211	6	kbr	kbr	PROPN
eurjchem-336	211	7	,	,	PUNCT
eurjchem-336	211	8			PROPN
eurjchem-336	211	9	,	,	PUNCT
eurjchem-336	211	10	cm‐1	cm‐1	PROPN
eurjchem-336	211	11	):	):	PUNCT
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eurjchem-336	211	13	,	,	PUNCT
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eurjchem-336	211	15	.	.	PUNCT
eurjchem-336	212	1	1h	1h	NUM
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eurjchem-336	212	3	(	(	PUNCT
eurjchem-336	212	4	300	300	NUM
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eurjchem-336	212	6	,	,	PUNCT
eurjchem-336	212	7	cdcl3	cdcl3	NOUN
eurjchem-336	212	8	):	):	PUNCT
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eurjchem-336	212	10	(	(	PUNCT
eurjchem-336	212	11	d	d	PROPN
eurjchem-336	212	12	,	,	PUNCT
eurjchem-336	212	13	2h	2h	NUM
eurjchem-336	212	14	,	,	PUNCT
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eurjchem-336	212	16	=	=	SYM
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eurjchem-336	212	18	hz	hz	NOUN
eurjchem-336	212	19	)	)	PUNCT
eurjchem-336	212	20	,	,	PUNCT
eurjchem-336	212	21	5.11	5.11	NUM
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eurjchem-336	212	32	,	,	PUNCT
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eurjchem-336	212	35	d	d	PROPN
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eurjchem-336	212	37	1h	1h	NUM
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eurjchem-336	212	43	)	)	PUNCT
eurjchem-336	212	44	,	,	PUNCT
eurjchem-336	212	45	7.41	7.41	NUM
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eurjchem-336	212	47	t	t	PROPN
eurjchem-336	212	48	,	,	PUNCT
eurjchem-336	212	49	1h	1h	NUM
eurjchem-336	212	50	,	,	PUNCT
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eurjchem-336	212	52	=	=	SYM
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eurjchem-336	212	54	hz	hz	NOUN
eurjchem-336	212	55	)	)	PUNCT
eurjchem-336	212	56	,	,	PUNCT
eurjchem-336	212	57	7.51‐7.57	7.51‐7.57	NUM
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eurjchem-336	212	59	m	m	PROPN
eurjchem-336	212	60	,	,	PUNCT
eurjchem-336	212	61	4h	4h	NOUN
eurjchem-336	212	62	)	)	PUNCT
eurjchem-336	212	63	,	,	PUNCT
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eurjchem-336	212	66	d	d	PROPN
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eurjchem-336	212	68	2h	2h	NUM
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eurjchem-336	213	1	=	=	SYM
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eurjchem-336	213	3	hz	hz	NOUN
eurjchem-336	213	4	)	)	PUNCT
eurjchem-336	213	5	,	,	PUNCT
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eurjchem-336	213	8	s	s	PROPN
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eurjchem-336	213	17	1h	1h	NUM
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eurjchem-336	213	19	.	.	PUNCT
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eurjchem-336	214	3	(	(	PUNCT
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eurjchem-336	214	8	):	):	PUNCT
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eurjchem-336	214	24	,	,	PUNCT
eurjchem-336	214	25	128.0	128.0	NUM
eurjchem-336	214	26	,	,	PUNCT
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eurjchem-336	214	38	,	,	PUNCT
eurjchem-336	214	39	157.1	157.1	NUM
eurjchem-336	214	40	,	,	PUNCT
eurjchem-336	214	41	188.2	188.2	NUM
eurjchem-336	214	42	.	.	PUNCT
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eurjchem-336	215	8	):	):	PUNCT
eurjchem-336	215	9	372	372	NUM
eurjchem-336	215	10	(	(	PUNCT
eurjchem-336	215	11	m+	m+	NUM
eurjchem-336	215	12	)	)	PUNCT
eurjchem-336	215	13	.	.	PUNCT
eurjchem-336	216	1	anal	anal	PROPN
eurjchem-336	216	2	.	.	PUNCT
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eurjchem-336	216	4	.	.	PUNCT
eurjchem-336	217	1	for	for	ADP
eurjchem-336	217	2	c19h14n2o2cl2	c19h14n2o2cl2	NOUN
eurjchem-336	217	3	:	:	PUNCT
eurjchem-336	217	4	c	c	X
eurjchem-336	217	5	,	,	PUNCT
eurjchem-336	217	6	61.29	61.29	NUM
eurjchem-336	217	7	;	;	PUNCT
eurjchem-336	217	8	h	h	NOUN
eurjchem-336	217	9	,	,	PUNCT
eurjchem-336	217	10	3.76	3.76	NUM
eurjchem-336	217	11	;	;	PUNCT
eurjchem-336	217	12	n	n	CCONJ
eurjchem-336	217	13	,	,	PUNCT
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eurjchem-336	217	17	:	:	PUNCT
eurjchem-336	218	1	c	c	X
eurjchem-336	218	2	,	,	PUNCT
eurjchem-336	218	3	61.46	61.46	NUM
eurjchem-336	218	4	;	;	PUNCT
eurjchem-336	219	1	h	h	NOUN
eurjchem-336	219	2	,	,	PUNCT
eurjchem-336	219	3	3.66	3.66	NUM
eurjchem-336	219	4	;	;	PUNCT
eurjchem-336	219	5	n	n	CCONJ
eurjchem-336	219	6	,	,	PUNCT
eurjchem-336	219	7	7.68	7.68	NUM
eurjchem-336	219	8	%	%	NOUN
eurjchem-336	219	9	.	.	PUNCT
eurjchem-336	220	1	3‐(2‐(allyloxy)‐5,3‐dibromophenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	3‐(2‐(allyloxy)‐5,3‐dibromophenyl)‐1‐phenyl‐1h‐pyrazole‐4‐	NUM
eurjchem-336	220	2	carbaldehyde	carbaldehyde	NOUN
eurjchem-336	220	3	(	(	PUNCT
eurjchem-336	220	4	4e	4e	NOUN
eurjchem-336	220	5	):	):	PUNCT
eurjchem-336	220	6	yield	yield	NOUN
eurjchem-336	220	7	:	:	PUNCT
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eurjchem-336	220	10	.	.	PUNCT
eurjchem-336	221	1	m.p	m.p	PROPN
eurjchem-336	221	2	.	.	PROPN
eurjchem-336	221	3	:	:	PUNCT
eurjchem-336	222	1	118‐120	118‐120	NUM
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eurjchem-336	222	3	.	.	PUNCT
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eurjchem-336	222	5	(	(	PUNCT
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eurjchem-336	222	15	.	.	PUNCT
eurjchem-336	223	1	1h	1h	NUM
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eurjchem-336	223	3	(	(	PUNCT
eurjchem-336	223	4	300	300	NUM
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eurjchem-336	223	13	2h	2h	NUM
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eurjchem-336	223	15	j	j	PROPN
eurjchem-336	223	16	=	=	PROPN
eurjchem-336	223	17	6	6	NUM
eurjchem-336	223	18	hz	hz	NOUN
eurjchem-336	223	19	)	)	PUNCT
eurjchem-336	223	20	,	,	PUNCT
eurjchem-336	223	21	5.02	5.02	NUM
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eurjchem-336	223	23	d	d	PROPN
eurjchem-336	223	24	,	,	PUNCT
eurjchem-336	223	25	1h	1h	NUM
eurjchem-336	223	26	,	,	PUNCT
eurjchem-336	223	27	j	j	PROPN
eurjchem-336	223	28	=	=	PROPN
eurjchem-336	223	29	10.5	10.5	NUM
eurjchem-336	223	30	hz	hz	NOUN
eurjchem-336	223	31	)	)	PUNCT
eurjchem-336	223	32	,	,	PUNCT
eurjchem-336	223	33	5.24	5.24	NUM
eurjchem-336	223	34	(	(	PUNCT
eurjchem-336	223	35	d	d	PROPN
eurjchem-336	223	36	,	,	PUNCT
eurjchem-336	223	37	1h	1h	NUM
eurjchem-336	223	38	,	,	PUNCT
eurjchem-336	223	39	j	j	PROPN
eurjchem-336	223	40	=	=	SYM
eurjchem-336	223	41	17	17	NUM
eurjchem-336	223	42	hz	hz	NOUN
eurjchem-336	223	43	)	)	PUNCT
eurjchem-336	223	44	,	,	PUNCT
eurjchem-336	223	45	7.45	7.45	NUM
eurjchem-336	223	46	(	(	PUNCT
eurjchem-336	223	47	t	t	PROPN
eurjchem-336	223	48	,	,	PUNCT
eurjchem-336	223	49	1h	1h	NUM
eurjchem-336	223	50	,	,	PUNCT
eurjchem-336	223	51	j	j	PROPN
eurjchem-336	223	52	=	=	SYM
eurjchem-336	223	53	7.5	7.5	NUM
eurjchem-336	223	54	hz	hz	NOUN
eurjchem-336	223	55	)	)	PUNCT
eurjchem-336	223	56	,	,	PUNCT
eurjchem-336	223	57	7.51	7.51	NUM
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eurjchem-336	223	59	d	d	PROPN
eurjchem-336	223	60	,	,	PUNCT
eurjchem-336	223	61	1h	1h	NUM
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eurjchem-336	223	67	)	)	PUNCT
eurjchem-336	223	68	,	,	PUNCT
eurjchem-336	223	69	7.53‐7.61	7.53‐7.61	NUM
eurjchem-336	223	70	(	(	PUNCT
eurjchem-336	223	71	m	m	PROPN
eurjchem-336	223	72	,	,	PUNCT
eurjchem-336	223	73	3h	3h	NUM
eurjchem-336	223	74	)	)	PUNCT
eurjchem-336	223	75	,	,	PUNCT
eurjchem-336	223	76	7.78	7.78	NUM
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eurjchem-336	223	78	d	d	PROPN
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eurjchem-336	223	80	2h	2h	NUM
eurjchem-336	223	81	,	,	PUNCT
eurjchem-336	223	82	j	j	PROPN
eurjchem-336	223	83	=	=	SYM
eurjchem-336	223	84	7.5	7.5	NUM
eurjchem-336	223	85	hz	hz	NOUN
eurjchem-336	223	86	)	)	PUNCT
eurjchem-336	223	87	,	,	PUNCT
eurjchem-336	223	88	8.54	8.54	NUM
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eurjchem-336	223	90	s	s	PROPN
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eurjchem-336	223	92	1h	1h	NUM
eurjchem-336	223	93	)	)	PUNCT
eurjchem-336	223	94	,	,	PUNCT
eurjchem-336	223	95	9.84	9.84	NUM
eurjchem-336	223	96	(	(	PUNCT
eurjchem-336	223	97	s	s	PROPN
eurjchem-336	223	98	,	,	PUNCT
eurjchem-336	223	99	1h	1h	NUM
eurjchem-336	223	100	)	)	PUNCT
eurjchem-336	223	101	.	.	PUNCT
eurjchem-336	224	1	13c	13c	NOUN
eurjchem-336	224	2	nmr	nmr	NOUN
eurjchem-336	224	3	(	(	PUNCT
eurjchem-336	224	4	75	75	NUM
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eurjchem-336	224	6	,	,	PUNCT
eurjchem-336	224	7	cdcl3	cdcl3	NOUN
eurjchem-336	224	8	):	):	PUNCT
eurjchem-336	224	9	68.8	68.8	NUM
eurjchem-336	224	10	,	,	PUNCT
eurjchem-336	224	11	112.0	112.0	NUM
eurjchem-336	224	12	,	,	PUNCT
eurjchem-336	224	13	115.4	115.4	NUM
eurjchem-336	224	14	,	,	PUNCT
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eurjchem-336	224	16	,	,	PUNCT
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eurjchem-336	224	18	,	,	PUNCT
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eurjchem-336	224	20	,	,	PUNCT
eurjchem-336	224	21	126.4	126.4	NUM
eurjchem-336	224	22	,	,	PUNCT
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eurjchem-336	224	24	,	,	PUNCT
eurjchem-336	224	25	130.0	130.0	NUM
eurjchem-336	224	26	,	,	PUNCT
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eurjchem-336	224	28	,	,	PUNCT
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eurjchem-336	224	32	,	,	PUNCT
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eurjchem-336	224	34	,	,	PUNCT
eurjchem-336	224	35	143.1	143.1	NUM
eurjchem-336	224	36	,	,	PUNCT
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eurjchem-336	224	38	,	,	PUNCT
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eurjchem-336	224	40	,	,	PUNCT
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eurjchem-336	224	42	.	.	PUNCT
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eurjchem-336	225	2	(	(	PUNCT
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eurjchem-336	225	7	z	z	NOUN
eurjchem-336	225	8	):	):	PUNCT
eurjchem-336	225	9	464	464	NUM
eurjchem-336	225	10	(	(	PUNCT
eurjchem-336	225	11	m+4	m+4	PROPN
eurjchem-336	225	12	)	)	PUNCT
eurjchem-336	225	13	,	,	PUNCT
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eurjchem-336	225	15	(	(	PUNCT
eurjchem-336	225	16	m+2	m+2	NOUN
eurjchem-336	225	17	)	)	PUNCT
eurjchem-336	225	18	,	,	PUNCT
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eurjchem-336	225	20	(	(	PUNCT
eurjchem-336	225	21	m+	m+	NUM
eurjchem-336	225	22	)	)	PUNCT
eurjchem-336	225	23	.	.	PUNCT
eurjchem-336	226	1	anal	anal	PROPN
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eurjchem-336	226	4	.	.	PUNCT
eurjchem-336	227	1	for	for	ADP
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eurjchem-336	227	4	c	c	X
eurjchem-336	227	5	,	,	PUNCT
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eurjchem-336	227	7	;	;	PUNCT
eurjchem-336	227	8	h	h	NOUN
eurjchem-336	227	9	,	,	PUNCT
eurjchem-336	227	10	3.04	3.04	NUM
eurjchem-336	227	11	;	;	PUNCT
eurjchem-336	227	12	n	n	CCONJ
eurjchem-336	227	13	,	,	PUNCT
eurjchem-336	227	14	6.08	6.08	NUM
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eurjchem-336	227	17	:	:	PUNCT
eurjchem-336	228	1	c	c	X
eurjchem-336	228	2	,	,	PUNCT
eurjchem-336	228	3	49.14	49.14	NUM
eurjchem-336	228	4	;	;	PUNCT
eurjchem-336	228	5	h	h	NOUN
eurjchem-336	228	6	,	,	PUNCT
eurjchem-336	228	7	3.12	3.12	NUM
eurjchem-336	228	8	;	;	PUNCT
eurjchem-336	228	9	n	n	CCONJ
eurjchem-336	228	10	,	,	PUNCT
eurjchem-336	228	11	6.26	6.26	NUM
eurjchem-336	228	12	%	%	NOUN
eurjchem-336	228	13	.	.	PUNCT
eurjchem-336	229	1	3‐(2‐(allyloxy)‐3‐bromo‐5‐chlorophenyl)‐1‐phenyl‐1h‐	3‐(2‐(allyloxy)‐3‐bromo‐5‐chlorophenyl)‐1‐phenyl‐1h‐	NUM
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eurjchem-336	229	3	(	(	PUNCT
eurjchem-336	229	4	4f	4f	NUM
eurjchem-336	229	5	):	):	PUNCT
eurjchem-336	229	6	yield	yield	NOUN
eurjchem-336	229	7	:	:	PUNCT
eurjchem-336	229	8	89	89	NUM
eurjchem-336	229	9	%	%	NOUN
eurjchem-336	229	10	.	.	PUNCT
eurjchem-336	230	1	m.p	m.p	PROPN
eurjchem-336	230	2	.	.	PROPN
eurjchem-336	230	3	:	:	PUNCT
eurjchem-336	231	1	112‐114	112‐114	NUM
eurjchem-336	231	2	oc	oc	PROPN
eurjchem-336	231	3	.	.	PUNCT
eurjchem-336	231	4	ft‐	ft‐	PROPN
eurjchem-336	231	5	ir	ir	PROPN
eurjchem-336	231	6	(	(	PUNCT
eurjchem-336	231	7	kbr	kbr	PROPN
eurjchem-336	231	8	,	,	PUNCT
eurjchem-336	231	9			PROPN
eurjchem-336	231	10	,	,	PUNCT
eurjchem-336	231	11	cm‐1	cm‐1	PROPN
eurjchem-336	231	12	):	):	PUNCT
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eurjchem-336	231	14	,	,	PUNCT
eurjchem-336	231	15	1604	1604	NUM
eurjchem-336	231	16	.	.	PUNCT
eurjchem-336	232	1	1h	1h	NUM
eurjchem-336	232	2	nmr	nmr	NOUN
eurjchem-336	232	3	(	(	PUNCT
eurjchem-336	232	4	300	300	NUM
eurjchem-336	232	5	mhz	mhz	NOUN
eurjchem-336	232	6	,	,	PUNCT
eurjchem-336	232	7	cdcl3	cdcl3	NOUN
eurjchem-336	232	8	):	):	PUNCT
eurjchem-336	232	9	4.31	4.31	NUM
eurjchem-336	232	10	(	(	PUNCT
eurjchem-336	232	11	d	d	NOUN
eurjchem-336	232	12	,	,	PUNCT
eurjchem-336	232	13	2h	2h	NUM
eurjchem-336	232	14	,	,	PUNCT
eurjchem-336	232	15	j	j	PROPN
eurjchem-336	232	16	=	=	SYM
eurjchem-336	232	17	5.7	5.7	NUM
eurjchem-336	232	18	hz	hz	NOUN
eurjchem-336	232	19	)	)	PUNCT
eurjchem-336	232	20	,	,	PUNCT
eurjchem-336	232	21	5.14	5.14	NUM
eurjchem-336	232	22	(	(	PUNCT
eurjchem-336	232	23	d	d	PROPN
eurjchem-336	232	24	,	,	PUNCT
eurjchem-336	232	25	1h	1h	NUM
eurjchem-336	232	26	,	,	PUNCT
eurjchem-336	232	27	j	j	PROPN
eurjchem-336	232	28	=	=	PROPN
eurjchem-336	232	29	10.4	10.4	NUM
eurjchem-336	232	30	hz	hz	NOUN
eurjchem-336	232	31	)	)	PUNCT
eurjchem-336	232	32	,	,	PUNCT
eurjchem-336	232	33	5.21	5.21	NUM
eurjchem-336	232	34	(	(	PUNCT
eurjchem-336	232	35	d	d	PROPN
eurjchem-336	232	36	,	,	PUNCT
eurjchem-336	232	37	1h	1h	NUM
eurjchem-336	232	38	,	,	PUNCT
eurjchem-336	232	39	j	j	PROPN
eurjchem-336	232	40	=	=	PROPN
eurjchem-336	232	41	17.8	17.8	NUM
eurjchem-336	232	42	hz	hz	NOUN
eurjchem-336	232	43	)	)	PUNCT
eurjchem-336	232	44	,	,	PUNCT
eurjchem-336	232	45	7.43	7.43	NUM
eurjchem-336	232	46	(	(	PUNCT
eurjchem-336	232	47	t	t	PROPN
eurjchem-336	232	48	,	,	PUNCT
eurjchem-336	232	49	1h	1h	NUM
eurjchem-336	232	50	,	,	PUNCT
eurjchem-336	232	51	j	j	PROPN
eurjchem-336	232	52	=	=	PROPN
eurjchem-336	232	53	7.6	7.6	NUM
eurjchem-336	232	54	hz	hz	NOUN
eurjchem-336	232	55	)	)	PUNCT
eurjchem-336	232	56	,	,	PUNCT
eurjchem-336	232	57	7.53‐7.59	7.53‐7.59	NUM
eurjchem-336	232	58	(	(	PUNCT
eurjchem-336	232	59	m	m	PROPN
eurjchem-336	232	60	,	,	PUNCT
eurjchem-336	232	61	4h	4h	NOUN
eurjchem-336	232	62	)	)	PUNCT
eurjchem-336	232	63	,	,	PUNCT
eurjchem-336	232	64	7.81	7.81	NUM
eurjchem-336	232	65	(	(	PUNCT
eurjchem-336	232	66	d	d	PROPN
eurjchem-336	232	67	,	,	PUNCT
eurjchem-336	232	68	2h	2h	NUM
eurjchem-336	232	69	,	,	PUNCT
eurjchem-336	232	70	j	j	PROPN
eurjchem-336	232	71	=	=	SYM
eurjchem-336	232	72	7.8	7.8	NUM
eurjchem-336	232	73	hz	hz	NOUN
eurjchem-336	232	74	)	)	PUNCT
eurjchem-336	232	75	,	,	PUNCT
eurjchem-336	232	76	8.59	8.59	NUM
eurjchem-336	232	77	(	(	PUNCT
eurjchem-336	232	78	s	s	PROPN
eurjchem-336	232	79	,	,	PUNCT
eurjchem-336	232	80	1h	1h	NUM
eurjchem-336	232	81	)	)	PUNCT
eurjchem-336	232	82	,	,	PUNCT
eurjchem-336	232	83	9.87	9.87	NUM
eurjchem-336	232	84	(	(	PUNCT
eurjchem-336	232	85	s	s	PROPN
eurjchem-336	232	86	,	,	PUNCT
eurjchem-336	232	87	1h	1h	NUM
eurjchem-336	232	88	)	)	PUNCT
eurjchem-336	232	89	.	.	PUNCT
eurjchem-336	233	1	13c	13c	NOUN
eurjchem-336	233	2	nmr	nmr	NOUN
eurjchem-336	233	3	(	(	PUNCT
eurjchem-336	233	4	75	75	NUM
eurjchem-336	233	5	m	m	NOUN
eurjchem-336	233	6	hz	hz	ADJ
eurjchem-336	233	7	,	,	PUNCT
eurjchem-336	233	8	cdcl3	cdcl3	NOUN
eurjchem-336	233	9	):	):	PUNCT
eurjchem-336	233	10	74.9	74.9	NUM
eurjchem-336	233	11	,	,	PUNCT
eurjchem-336	233	12	116.7	116.7	NUM
eurjchem-336	233	13	,	,	PUNCT
eurjchem-336	233	14	118.6	118.6	NUM
eurjchem-336	233	15	,	,	PUNCT
eurjchem-336	233	16	118.8	118.8	NUM
eurjchem-336	233	17	,	,	PUNCT
eurjchem-336	233	18	119.5	119.5	NUM
eurjchem-336	233	19	,	,	PUNCT
eurjchem-336	233	20	122.9	122.9	NUM
eurjchem-336	233	21	,	,	PUNCT
eurjchem-336	233	22	128.0	128.0	NUM
eurjchem-336	233	23	,	,	PUNCT
eurjchem-336	233	24	128.3	128.3	NUM
eurjchem-336	233	25	,	,	PUNCT
eurjchem-336	233	26	129.3	129.3	NUM
eurjchem-336	233	27	,	,	PUNCT
eurjchem-336	233	28	129.6	129.6	NUM
eurjchem-336	233	29	,	,	PUNCT
eurjchem-336	233	30	130.2	130.2	NUM
eurjchem-336	233	31	,	,	PUNCT
eurjchem-336	233	32	132.2	132.2	NUM
eurjchem-336	233	33	,	,	PUNCT
eurjchem-336	233	34	133.8	133.8	NUM
eurjchem-336	233	35	,	,	PUNCT
eurjchem-336	233	36	138.8	138.8	NUM
eurjchem-336	233	37	,	,	PUNCT
eurjchem-336	233	38	149.7	149.7	NUM
eurjchem-336	233	39	,	,	PUNCT
eurjchem-336	233	40	152.4	152.4	NUM
eurjchem-336	233	41	,	,	PUNCT
eurjchem-336	233	42	185.8	185.8	NUM
eurjchem-336	233	43	.	.	PUNCT
eurjchem-336	234	1	ms	ms	PROPN
eurjchem-336	234	2	(	(	PUNCT
eurjchem-336	234	3	ei	ei	PROPN
eurjchem-336	234	4	,	,	PUNCT
eurjchem-336	234	5	m	m	PROPN
eurjchem-336	234	6	/	/	SYM
eurjchem-336	234	7	z	z	NOUN
eurjchem-336	234	8	):	):	PUNCT
eurjchem-336	234	9	420	420	NUM
eurjchem-336	234	10	(	(	PUNCT
eurjchem-336	234	11	m+4	m+4	PROPN
eurjchem-336	234	12	)	)	PUNCT
eurjchem-336	234	13	,	,	PUNCT
eurjchem-336	234	14	418	418	NUM
eurjchem-336	234	15	(	(	PUNCT
eurjchem-336	234	16	m+2	m+2	NOUN
eurjchem-336	234	17	)	)	PUNCT
eurjchem-336	234	18	,	,	PUNCT
eurjchem-336	234	19	416	416	NUM
eurjchem-336	234	20	(	(	PUNCT
eurjchem-336	234	21	m+	m+	NUM
eurjchem-336	234	22	)	)	PUNCT
eurjchem-336	234	23	.	.	PUNCT
eurjchem-336	235	1	anal	anal	PROPN
eurjchem-336	235	2	.	.	PUNCT
eurjchem-336	235	3	calcd	calcd	NOUN
eurjchem-336	235	4	.	.	PUNCT
eurjchem-336	236	1	for	for	ADP
eurjchem-336	236	2	c19h14n2o2brcl	c19h14n2o2brcl	NOUN
eurjchem-336	236	3	:	:	PUNCT
eurjchem-336	236	4	c	c	X
eurjchem-336	236	5	,	,	PUNCT
eurjchem-336	236	6	54.80	54.80	NUM
eurjchem-336	236	7	;	;	PUNCT
eurjchem-336	236	8	h	h	NOUN
eurjchem-336	236	9	,	,	PUNCT
eurjchem-336	236	10	3.36	3.36	NUM
eurjchem-336	236	11	;	;	PUNCT
eurjchem-336	236	12	n	n	CCONJ
eurjchem-336	236	13	,	,	PUNCT
eurjchem-336	236	14	6.73	6.73	NUM
eurjchem-336	236	15	.	.	PUNCT
eurjchem-336	236	16	found	find	VERB
eurjchem-336	236	17	:	:	PUNCT
eurjchem-336	237	1	c	c	X
eurjchem-336	237	2	,	,	PUNCT
eurjchem-336	237	3	55.03	55.03	NUM
eurjchem-336	237	4	;	;	PUNCT
eurjchem-336	238	1	h	h	NOUN
eurjchem-336	238	2	,	,	PUNCT
eurjchem-336	238	3	3.40	3.40	NUM
eurjchem-336	238	4	;	;	PUNCT
eurjchem-336	238	5	n	n	CCONJ
eurjchem-336	238	6	,	,	PUNCT
eurjchem-336	238	7	6.51	6.51	NUM
eurjchem-336	238	8	%	%	NOUN
eurjchem-336	238	9	.	.	PUNCT
eurjchem-336	239	1	3‐(2‐(allyloxy)‐3‐bromo‐5‐methylphenyl)‐1‐phenyl‐1h‐	3‐(2‐(allyloxy)‐3‐bromo‐5‐methylphenyl)‐1‐phenyl‐1h‐	NUM
eurjchem-336	239	2	pyrazole‐4‐carbaldehyde	pyrazole‐4‐carbaldehyde	NUM
eurjchem-336	239	3	(	(	PUNCT
eurjchem-336	239	4	4	4	NUM
eurjchem-336	239	5	g	g	NOUN
eurjchem-336	239	6	):	):	PUNCT
eurjchem-336	239	7	yield	yield	NOUN
eurjchem-336	239	8	:	:	PUNCT
eurjchem-336	239	9	91	91	NUM
eurjchem-336	239	10	%	%	NOUN
eurjchem-336	239	11	.	.	PUNCT
eurjchem-336	240	1	m.p	m.p	PROPN
eurjchem-336	240	2	.	.	PROPN
eurjchem-336	240	3	:	:	PUNCT
eurjchem-336	241	1	102‐104	102‐104	NUM
eurjchem-336	241	2	oc	oc	AUX
eurjchem-336	241	3	.	.	PUNCT
eurjchem-336	241	4	ft‐	ft‐	PROPN
eurjchem-336	241	5	ir	ir	PROPN
eurjchem-336	241	6	(	(	PUNCT
eurjchem-336	241	7	kbr	kbr	PROPN
eurjchem-336	241	8	,	,	PUNCT
eurjchem-336	241	9			PROPN
eurjchem-336	241	10	,	,	PUNCT
eurjchem-336	241	11	cm‐1	cm‐1	PROPN
eurjchem-336	241	12	):	):	PUNCT
eurjchem-336	241	13	1672	1672	NUM
eurjchem-336	241	14	,	,	PUNCT
eurjchem-336	241	15	1614	1614	NUM
eurjchem-336	241	16	.	.	PUNCT
eurjchem-336	242	1	1h	1h	NUM
eurjchem-336	242	2	nmr	nmr	NOUN
eurjchem-336	242	3	(	(	PUNCT
eurjchem-336	242	4	300	300	NUM
eurjchem-336	242	5	mhz	mhz	NOUN
eurjchem-336	242	6	,	,	PUNCT
eurjchem-336	242	7	cdcl3	cdcl3	NOUN
eurjchem-336	242	8	):	):	PUNCT
eurjchem-336	242	9	2.38	2.38	NUM
eurjchem-336	242	10	(	(	PUNCT
eurjchem-336	242	11	s	s	PROPN
eurjchem-336	242	12	,	,	PUNCT
eurjchem-336	242	13	3h	3h	NUM
eurjchem-336	242	14	)	)	PUNCT
eurjchem-336	242	15	,	,	PUNCT
eurjchem-336	242	16	4.24	4.24	NUM
eurjchem-336	242	17	(	(	PUNCT
eurjchem-336	242	18	d	d	PROPN
eurjchem-336	242	19	,	,	PUNCT
eurjchem-336	242	20	2h	2h	NUM
eurjchem-336	242	21	,	,	PUNCT
eurjchem-336	242	22	j	j	PROPN
eurjchem-336	242	23	=	=	PROPN
eurjchem-336	242	24	6	6	NUM
eurjchem-336	242	25	hz	hz	NOUN
eurjchem-336	242	26	)	)	PUNCT
eurjchem-336	242	27	,	,	PUNCT
eurjchem-336	242	28	5.09	5.09	NUM
eurjchem-336	242	29	(	(	PUNCT
eurjchem-336	242	30	d	d	PROPN
eurjchem-336	242	31	,	,	PUNCT
eurjchem-336	242	32	1h	1h	NUM
eurjchem-336	242	33	,	,	PUNCT
eurjchem-336	242	34	j	j	PROPN
eurjchem-336	242	35	=	=	PROPN
eurjchem-336	242	36	10.8	10.8	NUM
eurjchem-336	242	37	hz	hz	NOUN
eurjchem-336	242	38	)	)	PUNCT
eurjchem-336	242	39	,	,	PUNCT
eurjchem-336	242	40	5.18	5.18	NUM
eurjchem-336	242	41	(	(	PUNCT
eurjchem-336	242	42	d	d	PROPN
eurjchem-336	242	43	,	,	PUNCT
eurjchem-336	242	44	1h	1h	NUM
eurjchem-336	242	45	,	,	PUNCT
eurjchem-336	242	46	j	j	PROPN
eurjchem-336	242	47	=	=	PROPN
eurjchem-336	242	48	16.8	16.8	NUM
eurjchem-336	242	49	hz	hz	NOUN
eurjchem-336	242	50	)	)	PUNCT
eurjchem-336	242	51	,	,	PUNCT
eurjchem-336	242	52	5.81	5.81	NUM
eurjchem-336	242	53	(	(	PUNCT
eurjchem-336	242	54	m	m	PROPN
eurjchem-336	242	55	,	,	PUNCT
eurjchem-336	242	56	1h	1h	NUM
eurjchem-336	242	57	)	)	PUNCT
eurjchem-336	242	58	,	,	PUNCT
eurjchem-336	242	59	7.40‐7.42	7.40‐7.42	NUM
eurjchem-336	242	60	(	(	PUNCT
eurjchem-336	242	61	m	m	PROPN
eurjchem-336	242	62	,	,	PUNCT
eurjchem-336	242	63	2h	2h	NUM
eurjchem-336	242	64	)	)	PUNCT
eurjchem-336	242	65	,	,	PUNCT
eurjchem-336	242	66	7.49‐7.54	7.49‐7.54	X
eurjchem-336	242	67	(	(	PUNCT
eurjchem-336	242	68	m	m	PROPN
eurjchem-336	242	69	,	,	PUNCT
eurjchem-336	242	70	2h	2h	NUM
eurjchem-336	242	71	)	)	PUNCT
eurjchem-336	242	72	,	,	PUNCT
eurjchem-336	242	73	7.78	7.78	NUM
eurjchem-336	242	74	(	(	PUNCT
eurjchem-336	242	75	d	d	PROPN
eurjchem-336	242	76	,	,	PUNCT
eurjchem-336	242	77	2h	2h	NUM
eurjchem-336	242	78	,	,	PUNCT
eurjchem-336	242	79	j	j	PROPN
eurjchem-336	242	80	=	=	SYM
eurjchem-336	242	81	8.1	8.1	NUM
eurjchem-336	242	82	hz	hz	NOUN
eurjchem-336	242	83	)	)	PUNCT
eurjchem-336	242	84	,	,	PUNCT
eurjchem-336	242	85	8.53	8.53	NUM
eurjchem-336	242	86	(	(	PUNCT
eurjchem-336	242	87	s	s	PROPN
eurjchem-336	242	88	,	,	PUNCT
eurjchem-336	242	89	1h	1h	NUM
eurjchem-336	242	90	)	)	PUNCT
eurjchem-336	242	91	,	,	PUNCT
eurjchem-336	242	92	9.84	9.84	NUM
eurjchem-336	242	93	(	(	PUNCT
eurjchem-336	242	94	s	s	PROPN
eurjchem-336	242	95	,	,	PUNCT
eurjchem-336	242	96	1h	1h	NUM
eurjchem-336	242	97	)	)	PUNCT
eurjchem-336	242	98	.	.	PUNCT
eurjchem-336	243	1	13c	13c	NOUN
eurjchem-336	243	2	nmr	nmr	NOUN
eurjchem-336	243	3	(	(	PUNCT
eurjchem-336	243	4	75	75	NUM
eurjchem-336	243	5	m	m	NOUN
eurjchem-336	243	6	hz	hz	ADJ
eurjchem-336	243	7	,	,	PUNCT
eurjchem-336	243	8	cdcl3	cdcl3	NOUN
eurjchem-336	243	9	):	):	PUNCT
eurjchem-336	243	10	24.1	24.1	NUM
eurjchem-336	243	11	,	,	PUNCT
eurjchem-336	243	12	69.3	69.3	NUM
eurjchem-336	243	13	,	,	PUNCT
eurjchem-336	243	14	114.3	114.3	NUM
eurjchem-336	243	15	,	,	PUNCT
eurjchem-336	243	16	115.1	115.1	NUM
eurjchem-336	243	17	,	,	PUNCT
eurjchem-336	243	18	119.4	119.4	NUM
eurjchem-336	243	19	,	,	PUNCT
eurjchem-336	243	20	119.8	119.8	NUM
eurjchem-336	243	21	,	,	PUNCT
eurjchem-336	243	22	123.2	123.2	NUM
eurjchem-336	243	23	,	,	PUNCT
eurjchem-336	243	24	128.3	128.3	NUM
eurjchem-336	243	25	,	,	PUNCT
eurjchem-336	243	26	129.6	129.6	NUM
eurjchem-336	243	27	,	,	PUNCT
eurjchem-336	243	28	131.4	131.4	NUM
eurjchem-336	243	29	,	,	PUNCT
eurjchem-336	243	30	131.5	131.5	NUM
eurjchem-336	243	31	,	,	PUNCT
eurjchem-336	243	32	134.0	134.0	NUM
eurjchem-336	243	33	,	,	PUNCT
eurjchem-336	243	34	134.7	134.7	NUM
eurjchem-336	243	35	,	,	PUNCT
eurjchem-336	243	36	134.9	134.9	NUM
eurjchem-336	243	37	,	,	PUNCT
eurjchem-336	243	38	139.9	139.9	NUM
eurjchem-336	243	39	,	,	PUNCT
eurjchem-336	243	40	150.8	150.8	NUM
eurjchem-336	243	41	,	,	PUNCT
eurjchem-336	243	42	156.2	156.2	NUM
eurjchem-336	243	43	,	,	PUNCT
eurjchem-336	243	44	184.8	184.8	NUM
eurjchem-336	243	45	.	.	PUNCT
eurjchem-336	244	1	ms	ms	NOUN
eurjchem-336	244	2	(	(	PUNCT
eurjchem-336	244	3	ei	ei	PROPN
eurjchem-336	244	4	,	,	PUNCT
eurjchem-336	244	5	m	m	PROPN
eurjchem-336	244	6	/	/	SYM
eurjchem-336	244	7	z	z	NOUN
eurjchem-336	244	8	):	):	PUNCT
eurjchem-336	244	9	398	398	NUM
eurjchem-336	244	10	(	(	PUNCT
eurjchem-336	244	11	m+2	m+2	NOUN
eurjchem-336	244	12	)	)	PUNCT
eurjchem-336	244	13	,	,	PUNCT
eurjchem-336	244	14	396	396	NUM
eurjchem-336	244	15	(	(	PUNCT
eurjchem-336	244	16	m+	m+	NUM
eurjchem-336	244	17	)	)	PUNCT
eurjchem-336	244	18	.	.	PUNCT
eurjchem-336	245	1	anal	anal	PROPN
eurjchem-336	245	2	.	.	PUNCT
eurjchem-336	245	3	calcd	calcd	NOUN
eurjchem-336	245	4	.	.	PUNCT
eurjchem-336	246	1	for	for	ADP
eurjchem-336	246	2	c20h17n2o2br	c20h17n2o2br	PROPN
eurjchem-336	246	3	:	:	PUNCT
eurjchem-336	246	4	c	c	X
eurjchem-336	246	5	,	,	PUNCT
eurjchem-336	246	6	60.60	60.60	NUM
eurjchem-336	246	7	;	;	PUNCT
eurjchem-336	246	8	h	h	X
eurjchem-336	246	9	,	,	PUNCT
eurjchem-336	246	10	4.29	4.29	NUM
eurjchem-336	246	11	;	;	PUNCT
eurjchem-336	246	12	n	n	CCONJ
eurjchem-336	246	13	,	,	PUNCT
eurjchem-336	246	14	7.07	7.07	NUM
eurjchem-336	246	15	.	.	PUNCT
eurjchem-336	246	16	found	find	VERB
eurjchem-336	246	17	:	:	PUNCT
eurjchem-336	247	1	c	c	X
eurjchem-336	247	2	,	,	PUNCT
eurjchem-336	247	3	60.56	60.56	NUM
eurjchem-336	247	4	;	;	PUNCT
eurjchem-336	247	5	h	h	X
eurjchem-336	247	6	,	,	PUNCT
eurjchem-336	247	7	4.28	4.28	NUM
eurjchem-336	247	8	;	;	PUNCT
eurjchem-336	247	9	n	n	CCONJ
eurjchem-336	247	10	,	,	PUNCT
eurjchem-336	247	11	7.11	7.11	NUM
eurjchem-336	247	12	%	%	NOUN
eurjchem-336	247	13	.	.	PUNCT
eurjchem-336	248	1	2.2.5	2.2.5	X
eurjchem-336	248	2	.	.	PUNCT
eurjchem-336	248	3	general	general	ADJ
eurjchem-336	248	4	procedure	procedure	NOUN
eurjchem-336	248	5	for	for	ADP
eurjchem-336	248	6	the	the	DET
eurjchem-336	248	7	preparation	preparation	NOUN
eurjchem-336	248	8	of	of	ADP
eurjchem-336	248	9	substituted	substitute	VERB
eurjchem-336	248	10	of	of	ADP
eurjchem-336	248	11	2‐arylpyrazolo[4,3‐c]coumarin	2‐arylpyrazolo[4,3‐c]coumarin	NUM
eurjchem-336	248	12	derivatives	derivative	NOUN
eurjchem-336	248	13	(	(	PUNCT
eurjchem-336	248	14	5a‐g	5a‐g	NUM
eurjchem-336	248	15	)	)	PUNCT
eurjchem-336	248	16	to	to	ADP
eurjchem-336	248	17	a	a	DET
eurjchem-336	248	18	solution	solution	NOUN
eurjchem-336	248	19	of	of	ADP
eurjchem-336	248	20	3‐(2‐hydroxyaryl)‐1‐phenyl‐1h‐pyrazole‐	3‐(2‐hydroxyaryl)‐1‐phenyl‐1h‐pyrazole‐	NUM
eurjchem-336	248	21	4‐carbaldehydes	4‐carbaldehyde	NOUN
eurjchem-336	248	22	(	(	PUNCT
eurjchem-336	248	23	3a‐g	3a‐g	NOUN
eurjchem-336	248	24	)	)	PUNCT
eurjchem-336	248	25	(	(	PUNCT
eurjchem-336	248	26	1	1	NUM
eurjchem-336	248	27	mmol	mmol	NOUN
eurjchem-336	248	28	)	)	PUNCT
eurjchem-336	248	29	or	or	CCONJ
eurjchem-336	248	30	3‐(2‐(allyloxyaryl)‐1‐	3‐(2‐(allyloxyaryl)‐1‐	NUM
eurjchem-336	248	31	phenyl‐1h‐pyrazole‐4‐carbaldehydes	phenyl‐1h‐pyrazole‐4‐carbaldehyde	NOUN
eurjchem-336	248	32	(	(	PUNCT
eurjchem-336	248	33	4a‐g	4a‐g	NOUN
eurjchem-336	248	34	)	)	PUNCT
eurjchem-336	248	35	(	(	PUNCT
eurjchem-336	248	36	1	1	NUM
eurjchem-336	248	37	mmol	mmol	NOUN
eurjchem-336	248	38	)	)	PUNCT
eurjchem-336	248	39	in	in	ADP
eurjchem-336	248	40	dmso	dmso	NOUN
eurjchem-336	248	41	(	(	PUNCT
eurjchem-336	248	42	10	10	NUM
eurjchem-336	248	43	ml	ml	NOUN
eurjchem-336	248	44	)	)	PUNCT
eurjchem-336	248	45	,	,	PUNCT
eurjchem-336	248	46	iodine	iodine	NOUN
eurjchem-336	248	47	(	(	PUNCT
eurjchem-336	248	48	10	10	NUM
eurjchem-336	248	49	mol%	mol%	NOUN
eurjchem-336	248	50	)	)	PUNCT
eurjchem-336	248	51	and	and	CCONJ
eurjchem-336	248	52	4‐5	4‐5	NOUN
eurjchem-336	248	53	drops	drop	NOUN
eurjchem-336	248	54	of	of	ADP
eurjchem-336	248	55	concentrated	concentrated	ADJ
eurjchem-336	248	56	h2so4	h2so4	PROPN
eurjchem-336	248	57	was	be	AUX
eurjchem-336	248	58	added	add	VERB
eurjchem-336	248	59	.	.	PUNCT
eurjchem-336	249	1	then	then	ADV
eurjchem-336	249	2	reaction	reaction	NOUN
eurjchem-336	249	3	mixture	mixture	NOUN
eurjchem-336	249	4	was	be	AUX
eurjchem-336	249	5	heated	heat	VERB
eurjchem-336	249	6	at	at	ADP
eurjchem-336	249	7	120	120	NUM
eurjchem-336	249	8	oc	oc	NOUN
eurjchem-336	249	9	.	.	PUNCT
eurjchem-336	250	1	after	after	ADP
eurjchem-336	250	2	the	the	DET
eurjchem-336	250	3	completion	completion	NOUN
eurjchem-336	250	4	of	of	ADP
eurjchem-336	250	5	the	the	DET
eurjchem-336	250	6	reaction	reaction	NOUN
eurjchem-336	250	7	(	(	PUNCT
eurjchem-336	250	8	checked	check	VERB
eurjchem-336	250	9	by	by	ADP
eurjchem-336	250	10	tlc	tlc	PROPN
eurjchem-336	250	11	)	)	PUNCT
eurjchem-336	250	12	,	,	PUNCT
eurjchem-336	250	13	the	the	DET
eurjchem-336	250	14	contents	content	NOUN
eurjchem-336	250	15	were	be	AUX
eurjchem-336	250	16	cooled	cool	VERB
eurjchem-336	250	17	to	to	ADP
eurjchem-336	250	18	room	room	NOUN
eurjchem-336	250	19	temperature	temperature	NOUN
eurjchem-336	250	20	and	and	CCONJ
eurjchem-336	250	21	poured	pour	VERB
eurjchem-336	250	22	into	into	ADP
eurjchem-336	250	23	ice‐	ice‐	PROPN
eurjchem-336	250	24	cooled	cooled	ADJ
eurjchem-336	250	25	water	water	NOUN
eurjchem-336	250	26	.	.	PUNCT
eurjchem-336	251	1	the	the	DET
eurjchem-336	251	2	separated	separate	VERB
eurjchem-336	251	3	solid	solid	ADJ
eurjchem-336	251	4	was	be	AUX
eurjchem-336	251	5	filtered	filter	VERB
eurjchem-336	251	6	and	and	CCONJ
eurjchem-336	251	7	washed	wash	VERB
eurjchem-336	251	8	with	with	ADP
eurjchem-336	251	9	cooled	cooled	ADJ
eurjchem-336	251	10	dilute	dilute	NOUN
eurjchem-336	251	11	sodium	sodium	NOUN
eurjchem-336	251	12	thiosulphate	thiosulphate	NOUN
eurjchem-336	251	13	solution	solution	NOUN
eurjchem-336	251	14	.	.	PUNCT
eurjchem-336	252	1	finally	finally	ADV
eurjchem-336	252	2	the	the	DET
eurjchem-336	252	3	obtained	obtain	VERB
eurjchem-336	252	4	product	product	NOUN
eurjchem-336	252	5	was	be	AUX
eurjchem-336	252	6	crystallized	crystallize	VERB
eurjchem-336	252	7	from	from	ADP
eurjchem-336	252	8	dmf	dmf	PROPN
eurjchem-336	252	9	to	to	PART
eurjchem-336	252	10	give	give	VERB
eurjchem-336	252	11	product	product	NOUN
eurjchem-336	252	12	5a‐g	5a‐g	NUM
eurjchem-336	252	13	.	.	PUNCT
eurjchem-336	253	1	8‐chloro‐2‐phenylchromeno[4,3‐c]pyrazol‐4(2h)‐one	8‐chloro‐2‐phenylchromeno[4,3‐c]pyrazol‐4(2h)‐one	NUM
eurjchem-336	253	2	(	(	PUNCT
eurjchem-336	253	3	5a	5a	NUM
eurjchem-336	253	4	):	):	PUNCT
eurjchem-336	253	5	ft‐ir	ft‐ir	NOUN
eurjchem-336	253	6	(	(	PUNCT
eurjchem-336	253	7	kbr	kbr	PROPN
eurjchem-336	253	8	,	,	PUNCT
eurjchem-336	253	9			PROPN
eurjchem-336	253	10	,	,	PUNCT
eurjchem-336	253	11	cm‐1	cm‐1	PROPN
eurjchem-336	253	12	):	):	PUNCT
eurjchem-336	253	13	1734	1734	NUM
eurjchem-336	253	14	.	.	PUNCT
eurjchem-336	254	1	1h	1h	NUM
eurjchem-336	254	2	nmr	nmr	NOUN
eurjchem-336	254	3	(	(	PUNCT
eurjchem-336	254	4	300	300	NUM
eurjchem-336	254	5	mhz	mhz	NOUN
eurjchem-336	254	6	,	,	PUNCT
eurjchem-336	254	7	dmso‐d6	dmso‐d6	NUM
eurjchem-336	254	8	):	):	PUNCT
eurjchem-336	254	9	7.35	7.35	NUM
eurjchem-336	254	10	(	(	PUNCT
eurjchem-336	254	11	d	d	PROPN
eurjchem-336	254	12	,	,	PUNCT
eurjchem-336	254	13	1h	1h	NUM
eurjchem-336	254	14	,	,	PUNCT
eurjchem-336	254	15	j	j	PROPN
eurjchem-336	254	16	=	=	SYM
eurjchem-336	254	17	8.7	8.7	NUM
eurjchem-336	254	18	hz	hz	NOUN
eurjchem-336	254	19	,	,	PUNCT
eurjchem-336	254	20	c6‐h	c6‐h	PROPN
eurjchem-336	254	21	)	)	PUNCT
eurjchem-336	254	22	,	,	PUNCT
eurjchem-336	254	23	7.44‐7.50	7.44‐7.50	PROPN
eurjchem-336	254	24	(	(	PUNCT
eurjchem-336	254	25	m	m	PROPN
eurjchem-336	254	26	,	,	PUNCT
eurjchem-336	254	27	2h	2h	NUM
eurjchem-336	254	28	,	,	PUNCT
eurjchem-336	254	29	c7‐h	c7‐h	PROPN
eurjchem-336	254	30	&	&	CCONJ
eurjchem-336	254	31	ph‐h	ph‐h	PROPN
eurjchem-336	254	32	)	)	PUNCT
eurjchem-336	254	33	,	,	PUNCT
eurjchem-336	254	34	7.57	7.57	NUM
eurjchem-336	254	35	(	(	PUNCT
eurjchem-336	254	36	t	t	PROPN
eurjchem-336	254	37	,	,	PUNCT
eurjchem-336	254	38	2h	2h	NUM
eurjchem-336	254	39	,	,	PUNCT
eurjchem-336	254	40	j	j	PROPN
eurjchem-336	254	41	=	=	SYM
eurjchem-336	254	42	7.8	7.8	NUM
eurjchem-336	254	43	hz	hz	NOUN
eurjchem-336	254	44	,	,	PUNCT
eurjchem-336	254	45	ph‐h	ph‐h	PROPN
eurjchem-336	254	46	)	)	PUNCT
eurjchem-336	254	47	,	,	PUNCT
eurjchem-336	254	48	7.84	7.84	NUM
eurjchem-336	254	49	(	(	PUNCT
eurjchem-336	254	50	d	d	PROPN
eurjchem-336	254	51	,	,	PUNCT
eurjchem-336	254	52	2h	2h	NUM
eurjchem-336	254	53	,	,	PUNCT
eurjchem-336	254	54	j	j	PROPN
eurjchem-336	254	55	=	=	PROPN
eurjchem-336	254	56	8.4	8.4	NUM
eurjchem-336	254	57	hz	hz	NOUN
eurjchem-336	254	58	,	,	PUNCT
eurjchem-336	254	59	ph‐h	ph‐h	PROPN
eurjchem-336	254	60	)	)	PUNCT
eurjchem-336	254	61	,	,	PUNCT
eurjchem-336	254	62	8.17	8.17	NUM
eurjchem-336	254	63	(	(	PUNCT
eurjchem-336	254	64	d	d	PROPN
eurjchem-336	254	65	,	,	PUNCT
eurjchem-336	254	66	1h	1h	NUM
eurjchem-336	254	67	,	,	PUNCT
eurjchem-336	254	68	j	j	PROPN
eurjchem-336	254	69	=	=	SYM
eurjchem-336	254	70	2.7	2.7	NUM
eurjchem-336	254	71	hz	hz	ADJ
eurjchem-336	254	72	,	,	PUNCT
eurjchem-336	254	73	c9‐h	c9‐h	NOUN
eurjchem-336	254	74	)	)	PUNCT
eurjchem-336	254	75	,	,	PUNCT
eurjchem-336	254	76	8.69	8.69	NUM
eurjchem-336	254	77	(	(	PUNCT
eurjchem-336	254	78	s	s	PROPN
eurjchem-336	254	79	,	,	PUNCT
eurjchem-336	254	80	1h	1h	NUM
eurjchem-336	254	81	,	,	PUNCT
eurjchem-336	254	82	c3‐h	c3‐h	PROPN
eurjchem-336	254	83	)	)	PUNCT
eurjchem-336	254	84	.	.	PUNCT
eurjchem-336	255	1	13c	13c	NOUN
eurjchem-336	255	2	nmr	nmr	NOUN
eurjchem-336	255	3	(	(	PUNCT
eurjchem-336	255	4	75	75	NUM
eurjchem-336	255	5	mhz	mhz	NOUN
eurjchem-336	255	6	,	,	PUNCT
eurjchem-336	255	7	dmso‐d6	dmso‐d6	NUM
eurjchem-336	255	8	):	):	PUNCT
eurjchem-336	255	9	109.1	109.1	NUM
eurjchem-336	255	10	,	,	PUNCT
eurjchem-336	255	11	116.3	116.3	NUM
eurjchem-336	255	12	,	,	PUNCT
eurjchem-336	255	13	120.8	120.8	NUM
eurjchem-336	255	14	,	,	PUNCT
eurjchem-336	255	15	125.9	125.9	NUM
eurjchem-336	255	16	,	,	PUNCT
eurjchem-336	255	17	127.1	127.1	NUM
eurjchem-336	255	18	,	,	PUNCT
eurjchem-336	255	19	127.9	127.9	NUM
eurjchem-336	255	20	,	,	PUNCT
eurjchem-336	255	21	128.9	128.9	NUM
eurjchem-336	255	22	,	,	PUNCT
eurjchem-336	255	23	129.1	129.1	NUM
eurjchem-336	255	24	,	,	PUNCT
eurjchem-336	255	25	130.9	130.9	NUM
eurjchem-336	255	26	,	,	PUNCT
eurjchem-336	255	27	132.2	132.2	NUM
eurjchem-336	255	28	,	,	PUNCT
eurjchem-336	255	29	140.2	140.2	NUM
eurjchem-336	255	30	,	,	PUNCT
eurjchem-336	255	31	150.1	150.1	NUM
eurjchem-336	255	32	,	,	PUNCT
eurjchem-336	255	33	150.9	150.9	NUM
eurjchem-336	255	34	,	,	PUNCT
eurjchem-336	255	35	157.7	157.7	NUM
eurjchem-336	255	36	.	.	PUNCT
eurjchem-336	256	1	ms	ms	PROPN
eurjchem-336	256	2	(	(	PUNCT
eurjchem-336	256	3	ei	ei	PROPN
eurjchem-336	256	4	,	,	PUNCT
eurjchem-336	256	5	m	m	PROPN
eurjchem-336	256	6	/	/	SYM
eurjchem-336	256	7	z	z	NOUN
eurjchem-336	256	8	):	):	PUNCT
eurjchem-336	256	9	296	296	NUM
eurjchem-336	256	10	(	(	PUNCT
eurjchem-336	256	11	m+	m+	NUM
eurjchem-336	256	12	)	)	PUNCT
eurjchem-336	256	13	.	.	PUNCT
eurjchem-336	257	1	anal	anal	PROPN
eurjchem-336	257	2	.	.	PUNCT
eurjchem-336	257	3	calcd	calcd	NOUN
eurjchem-336	257	4	.	.	PUNCT
eurjchem-336	258	1	for	for	ADP
eurjchem-336	258	2	c16h9n2o2cl	c16h9n2o2cl	PROPN
eurjchem-336	258	3	.	.	PUNCT
eurjchem-336	259	1	c	c	X
eurjchem-336	259	2	,	,	PUNCT
eurjchem-336	259	3	64.86	64.86	NUM
eurjchem-336	259	4	;	;	PUNCT
eurjchem-336	259	5	h	h	NOUN
eurjchem-336	259	6	,	,	PUNCT
eurjchem-336	259	7	3.04	3.04	NUM
eurjchem-336	259	8	;	;	PUNCT
eurjchem-336	259	9	n	n	CCONJ
eurjchem-336	259	10	,	,	PUNCT
eurjchem-336	259	11	9.45	9.45	NUM
eurjchem-336	259	12	.	.	PUNCT
eurjchem-336	259	13	found	find	VERB
eurjchem-336	259	14	:	:	PUNCT
eurjchem-336	260	1	c	c	X
eurjchem-336	260	2	,	,	PUNCT
eurjchem-336	260	3	63.94	63.94	NUM
eurjchem-336	260	4	;	;	PUNCT
eurjchem-336	260	5	h	h	NOUN
eurjchem-336	260	6	,	,	PUNCT
eurjchem-336	260	7	3.01	3.01	NUM
eurjchem-336	260	8	;	;	PUNCT
eurjchem-336	260	9	n	n	CCONJ
eurjchem-336	260	10	,	,	PUNCT
eurjchem-336	260	11	9.57	9.57	NUM
eurjchem-336	260	12	%	%	NOUN
eurjchem-336	260	13	.	.	PUNCT
eurjchem-336	261	1	8‐bromo‐2‐phenylchromeno[4,3‐c]pyrazol‐4(2h)‐one	8‐bromo‐2‐phenylchromeno[4,3‐c]pyrazol‐4(2h)‐one	NUM
eurjchem-336	261	2	(	(	PUNCT
eurjchem-336	261	3	5b	5b	NUM
eurjchem-336	261	4	):	):	PUNCT
eurjchem-336	261	5	ft‐ir	ft‐ir	NOUN
eurjchem-336	261	6	(	(	PUNCT
eurjchem-336	261	7	kbr	kbr	PROPN
eurjchem-336	261	8	,	,	PUNCT
eurjchem-336	261	9			PROPN
eurjchem-336	261	10	,	,	PUNCT
eurjchem-336	261	11	cm‐1	cm‐1	PROPN
eurjchem-336	261	12	):	):	PUNCT
eurjchem-336	261	13	1741	1741	NUM
eurjchem-336	261	14	.	.	PUNCT
eurjchem-336	262	1	1h	1h	NUM
eurjchem-336	262	2	nmr	nmr	NOUN
eurjchem-336	262	3	(	(	PUNCT
eurjchem-336	262	4	300	300	NUM
eurjchem-336	262	5	mhz	mhz	NOUN
eurjchem-336	262	6	,	,	PUNCT
eurjchem-336	262	7	dmso‐d6	dmso‐d6	NUM
eurjchem-336	262	8	):	):	PUNCT
eurjchem-336	262	9	7.38	7.38	NUM
eurjchem-336	262	10	(	(	PUNCT
eurjchem-336	262	11	d	d	PROPN
eurjchem-336	262	12	,	,	PUNCT
eurjchem-336	262	13	1h	1h	NUM
eurjchem-336	262	14	,	,	PUNCT
eurjchem-336	262	15	j	j	PROPN
eurjchem-336	262	16	=	=	SYM
eurjchem-336	262	17	8.1	8.1	NUM
eurjchem-336	262	18	hz	hz	VERB
eurjchem-336	262	19	,	,	PUNCT
eurjchem-336	262	20	c6‐h	c6‐h	PROPN
eurjchem-336	262	21	)	)	PUNCT
eurjchem-336	262	22	,	,	PUNCT
eurjchem-336	262	23	7.49‐7.54	7.49‐7.54	PROPN
eurjchem-336	262	24	(	(	PUNCT
eurjchem-336	262	25	m	m	PROPN
eurjchem-336	262	26	,	,	PUNCT
eurjchem-336	262	27	2h	2h	NUM
eurjchem-336	262	28	,	,	PUNCT
eurjchem-336	262	29	c7‐h	c7‐h	PROPN
eurjchem-336	262	30	&	&	CCONJ
eurjchem-336	262	31	ph‐h	ph‐h	PROPN
eurjchem-336	262	32	)	)	PUNCT
eurjchem-336	262	33	,	,	PUNCT
eurjchem-336	262	34	7.59	7.59	NUM
eurjchem-336	262	35	(	(	PUNCT
eurjchem-336	262	36	t	t	PROPN
eurjchem-336	262	37	,	,	PUNCT
eurjchem-336	262	38	2h	2h	NUM
eurjchem-336	262	39	,	,	PUNCT
eurjchem-336	262	40	j	j	PROPN
eurjchem-336	262	41	=	=	SYM
eurjchem-336	262	42	7.8	7.8	NUM
eurjchem-336	262	43	hz	hz	NOUN
eurjchem-336	262	44	,	,	PUNCT
eurjchem-336	262	45	ph‐h	ph‐h	PROPN
eurjchem-336	262	46	)	)	PUNCT
eurjchem-336	262	47	,	,	PUNCT
eurjchem-336	262	48	7.81	7.81	NUM
eurjchem-336	262	49	(	(	PUNCT
eurjchem-336	262	50	d	d	PROPN
eurjchem-336	262	51	,	,	PUNCT
eurjchem-336	262	52	2h	2h	NUM
eurjchem-336	262	53	,	,	PUNCT
eurjchem-336	262	54	j	j	PROPN
eurjchem-336	262	55	=	=	PROPN
eurjchem-336	262	56	8.4	8.4	NUM
eurjchem-336	262	57	hz	hz	NOUN
eurjchem-336	262	58	,	,	PUNCT
eurjchem-336	262	59	ph‐h	ph‐h	PROPN
eurjchem-336	262	60	)	)	PUNCT
eurjchem-336	262	61	,	,	PUNCT
eurjchem-336	262	62	8.35	8.35	NUM
eurjchem-336	262	63	(	(	PUNCT
eurjchem-336	262	64	d	d	PROPN
eurjchem-336	262	65	,	,	PUNCT
eurjchem-336	262	66	1h	1h	NUM
eurjchem-336	262	67	,	,	PUNCT
eurjchem-336	262	68	j	j	PROPN
eurjchem-336	262	69	=	=	SYM
eurjchem-336	262	70	2.9	2.9	NUM
eurjchem-336	262	71	hz	hz	ADJ
eurjchem-336	262	72	,	,	PUNCT
eurjchem-336	262	73	c9‐h	c9‐h	NOUN
eurjchem-336	262	74	)	)	PUNCT
eurjchem-336	262	75	,	,	PUNCT
eurjchem-336	262	76	8.71(s	8.71(s	PROPN
eurjchem-336	262	77	,	,	PUNCT
eurjchem-336	262	78	1h	1h	NUM
eurjchem-336	262	79	,	,	PUNCT
eurjchem-336	262	80	c3‐h	c3‐h	PROPN
eurjchem-336	262	81	)	)	PUNCT
eurjchem-336	262	82	.	.	PUNCT
eurjchem-336	263	1	13c	13c	NOUN
eurjchem-336	263	2	nmr	nmr	NOUN
eurjchem-336	263	3	(	(	PUNCT
eurjchem-336	263	4	75	75	NUM
eurjchem-336	263	5	mhz	mhz	NOUN
eurjchem-336	263	6	,	,	PUNCT
eurjchem-336	263	7	dmso‐d6	dmso‐d6	NUM
eurjchem-336	263	8	):	):	PUNCT
eurjchem-336	263	9	106.9	106.9	NUM
eurjchem-336	263	10	,	,	PUNCT
eurjchem-336	263	11	115.1	115.1	NUM
eurjchem-336	263	12	,	,	PUNCT
eurjchem-336	263	13	119.0	119.0	NUM
eurjchem-336	263	14	,	,	PUNCT
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eurjchem-336	263	16	,	,	PUNCT
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eurjchem-336	263	43	)	)	PUNCT
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eurjchem-336	264	8	):	):	PUNCT
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eurjchem-336	264	10	(	(	PUNCT
eurjchem-336	264	11	m+	m+	NUM
eurjchem-336	264	12	)	)	PUNCT
eurjchem-336	264	13	.	.	PUNCT
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eurjchem-336	265	2	.	.	PUNCT
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eurjchem-336	267	2	,	,	PUNCT
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eurjchem-336	268	1	h	h	X
eurjchem-336	268	2	,	,	PUNCT
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eurjchem-336	268	4	;	;	PUNCT
eurjchem-336	268	5	n	n	CCONJ
eurjchem-336	268	6	,	,	PUNCT
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eurjchem-336	270	1	c	c	X
eurjchem-336	270	2	,	,	PUNCT
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eurjchem-336	270	4	;	;	PUNCT
eurjchem-336	270	5	h	h	NOUN
eurjchem-336	270	6	,	,	PUNCT
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eurjchem-336	270	8	;	;	PUNCT
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eurjchem-336	270	10	,	,	PUNCT
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eurjchem-336	271	3	5c	5c	NUM
eurjchem-336	271	4	):	):	PUNCT
eurjchem-336	271	5	ft‐ir	ft‐ir	NOUN
eurjchem-336	271	6	(	(	PUNCT
eurjchem-336	271	7	kbr	kbr	PROPN
eurjchem-336	271	8	,	,	PUNCT
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eurjchem-336	271	10	,	,	PUNCT
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eurjchem-336	271	14	.	.	PUNCT
eurjchem-336	272	1	1h	1h	NUM
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eurjchem-336	272	3	(	(	PUNCT
eurjchem-336	272	4	300	300	NUM
eurjchem-336	272	5	mhz	mhz	NOUN
eurjchem-336	272	6	,	,	PUNCT
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eurjchem-336	272	8	):	):	PUNCT
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eurjchem-336	272	16	=	=	SYM
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eurjchem-336	272	19	,	,	PUNCT
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eurjchem-336	272	22	,	,	PUNCT
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eurjchem-336	272	26	,	,	PUNCT
eurjchem-336	272	27	2h	2h	NUM
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eurjchem-336	272	30	&	&	CCONJ
eurjchem-336	272	31	ph‐h	ph‐h	PROPN
eurjchem-336	272	32	)	)	PUNCT
eurjchem-336	272	33	,	,	PUNCT
eurjchem-336	272	34	7.60	7.60	NUM
eurjchem-336	272	35	(	(	PUNCT
eurjchem-336	272	36	t	t	PROPN
eurjchem-336	272	37	,	,	PUNCT
eurjchem-336	272	38	2h	2h	NUM
eurjchem-336	272	39	,	,	PUNCT
eurjchem-336	272	40	j	j	PROPN
eurjchem-336	272	41	=	=	SYM
eurjchem-336	272	42	8.1	8.1	NUM
eurjchem-336	272	43	hz	hz	NOUN
eurjchem-336	272	44	,	,	PUNCT
eurjchem-336	272	45	ph‐h	ph‐h	PROPN
eurjchem-336	272	46	)	)	PUNCT
eurjchem-336	272	47	,	,	PUNCT
eurjchem-336	272	48	7.84	7.84	NUM
eurjchem-336	272	49	(	(	PUNCT
eurjchem-336	272	50	d	d	PROPN
eurjchem-336	272	51	,	,	PUNCT
eurjchem-336	272	52	2h	2h	NUM
eurjchem-336	272	53	,	,	PUNCT
eurjchem-336	272	54	j	j	PROPN
eurjchem-336	272	55	=	=	PROPN
eurjchem-336	272	56	8.4	8.4	NUM
eurjchem-336	272	57	hz	hz	NOUN
eurjchem-336	272	58	,	,	PUNCT
eurjchem-336	272	59	ph‐h	ph‐h	PROPN
eurjchem-336	272	60	)	)	PUNCT
eurjchem-336	272	61	,	,	PUNCT
eurjchem-336	272	62	8.15	8.15	NUM
eurjchem-336	272	63	(	(	PUNCT
eurjchem-336	272	64	dd	dd	PROPN
eurjchem-336	272	65	,	,	PUNCT
eurjchem-336	272	66	1h	1h	NUM
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eurjchem-336	272	69	hz	hz	PROPN
eurjchem-336	272	70	,	,	PUNCT
eurjchem-336	272	71	j2=	j2=	PROPN
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eurjchem-336	272	74	,	,	PUNCT
eurjchem-336	272	75	c9‐h	c9‐h	NOUN
eurjchem-336	272	76	)	)	PUNCT
eurjchem-336	272	77	,	,	PUNCT
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eurjchem-336	272	81	,	,	PUNCT
eurjchem-336	272	82	1h	1h	NUM
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eurjchem-336	272	85	)	)	PUNCT
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eurjchem-336	273	1	13c	13c	NOUN
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eurjchem-336	273	3	(	(	PUNCT
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eurjchem-336	273	5	mhz	mhz	NOUN
eurjchem-336	273	6	,	,	PUNCT
eurjchem-336	273	7	dmso‐d6	dmso‐d6	NUM
eurjchem-336	273	8	):	):	PUNCT
eurjchem-336	273	9	105.1	105.1	NUM
eurjchem-336	273	10	,	,	PUNCT
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eurjchem-336	273	18	,	,	PUNCT
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eurjchem-336	273	20	,	,	PUNCT
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eurjchem-336	273	22	,	,	PUNCT
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eurjchem-336	273	24	,	,	PUNCT
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eurjchem-336	273	28	,	,	PUNCT
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eurjchem-336	273	30	,	,	PUNCT
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eurjchem-336	273	32	,	,	PUNCT
eurjchem-336	273	33	152.3	152.3	NUM
eurjchem-336	273	34	,	,	PUNCT
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eurjchem-336	273	36	.	.	PUNCT
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eurjchem-336	274	2	(	(	PUNCT
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eurjchem-336	274	8	):	):	PUNCT
eurjchem-336	274	9	296	296	NUM
eurjchem-336	274	10	(	(	PUNCT
eurjchem-336	274	11	m+	m+	NUM
eurjchem-336	274	12	)	)	PUNCT
eurjchem-336	274	13	.	.	PUNCT
eurjchem-336	275	1	anal	anal	PROPN
eurjchem-336	275	2	.	.	PUNCT
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eurjchem-336	275	4	.	.	PUNCT
eurjchem-336	276	1	for	for	ADP
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eurjchem-336	276	3	.	.	PUNCT
eurjchem-336	277	1	c	c	X
eurjchem-336	277	2	,	,	PUNCT
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eurjchem-336	277	4	;	;	PUNCT
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eurjchem-336	277	6	,	,	PUNCT
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eurjchem-336	277	8	;	;	PUNCT
eurjchem-336	277	9	n	n	CCONJ
eurjchem-336	277	10	,	,	PUNCT
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eurjchem-336	277	14	:	:	PUNCT
eurjchem-336	278	1	c	c	X
eurjchem-336	278	2	,	,	PUNCT
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eurjchem-336	278	4	;	;	PUNCT
eurjchem-336	278	5	h	h	NOUN
eurjchem-336	278	6	,	,	PUNCT
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eurjchem-336	278	8	;	;	PUNCT
eurjchem-336	278	9	n	n	CCONJ
eurjchem-336	278	10	,	,	PUNCT
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eurjchem-336	278	13	.	.	PUNCT
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eurjchem-336	279	3	(	(	PUNCT
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eurjchem-336	279	5	):	):	PUNCT
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eurjchem-336	279	7	(	(	PUNCT
eurjchem-336	279	8	kbr	kbr	PROPN
eurjchem-336	279	9	,	,	PUNCT
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eurjchem-336	279	13	):	):	PUNCT
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eurjchem-336	280	5	mhz	mhz	NOUN
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eurjchem-336	280	8	):	):	PUNCT
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eurjchem-336	280	12	,	,	PUNCT
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eurjchem-336	280	14	,	,	PUNCT
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eurjchem-336	280	16	=	=	SYM
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eurjchem-336	280	19	,	,	PUNCT
eurjchem-336	280	20	ph‐h	ph‐h	PROPN
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eurjchem-336	280	22	,	,	PUNCT
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eurjchem-336	280	30	&	&	CCONJ
eurjchem-336	280	31	ph‐h	ph‐h	PROPN
eurjchem-336	280	32	)	)	PUNCT
eurjchem-336	280	33	,	,	PUNCT
eurjchem-336	280	34	7.84	7.84	NUM
eurjchem-336	280	35	(	(	PUNCT
eurjchem-336	280	36	d	d	PROPN
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eurjchem-336	280	38	2h	2h	NUM
eurjchem-336	280	39	,	,	PUNCT
eurjchem-336	280	40	j	j	PROPN
eurjchem-336	280	41	=	=	SYM
eurjchem-336	280	42	7.8	7.8	NUM
eurjchem-336	280	43	hz	hz	NOUN
eurjchem-336	280	44	,	,	PUNCT
eurjchem-336	280	45	ph‐h	ph‐h	PROPN
eurjchem-336	280	46	)	)	PUNCT
eurjchem-336	280	47	,	,	PUNCT
eurjchem-336	280	48	8.10	8.10	NUM
eurjchem-336	280	49	(	(	PUNCT
eurjchem-336	280	50	d	d	PROPN
eurjchem-336	280	51	,	,	PUNCT
eurjchem-336	280	52	1h	1h	NUM
eurjchem-336	280	53	,	,	PUNCT
eurjchem-336	280	54	j	j	PROPN
eurjchem-336	280	55	=	=	SYM
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eurjchem-336	280	57	hz	hz	ADJ
eurjchem-336	280	58	,	,	PUNCT
eurjchem-336	280	59	c9‐h	c9‐h	NOUN
eurjchem-336	280	60	)	)	PUNCT
eurjchem-336	280	61	,	,	PUNCT
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eurjchem-336	281	3	(	(	PUNCT
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eurjchem-336	281	6	,	,	PUNCT
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eurjchem-336	281	8	):	):	PUNCT
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eurjchem-336	281	26	,	,	PUNCT
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eurjchem-336	281	28	,	,	PUNCT
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eurjchem-336	281	30	,	,	PUNCT
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eurjchem-336	281	36	.	.	PUNCT
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eurjchem-336	282	4	,	,	PUNCT
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eurjchem-336	282	7	z	z	NOUN
eurjchem-336	282	8	):	):	PUNCT
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eurjchem-336	282	10	(	(	PUNCT
eurjchem-336	282	11	m+	m+	NUM
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eurjchem-336	282	13	.	.	PUNCT
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eurjchem-336	283	4	.	.	PUNCT
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eurjchem-336	285	2	,	,	PUNCT
eurjchem-336	285	3	58.18	58.18	NUM
eurjchem-336	285	4	;	;	PUNCT
eurjchem-336	285	5	h	h	NOUN
eurjchem-336	285	6	,	,	PUNCT
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eurjchem-336	285	9	n	n	CCONJ
eurjchem-336	285	10	,	,	PUNCT
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eurjchem-336	285	14	:	:	PUNCT
eurjchem-336	286	1	c	c	X
eurjchem-336	286	2	,	,	PUNCT
eurjchem-336	286	3	58.34	58.34	NUM
eurjchem-336	286	4	;	;	PUNCT
eurjchem-336	286	5	h	h	NOUN
eurjchem-336	286	6	,	,	PUNCT
eurjchem-336	286	7	2.61	2.61	NUM
eurjchem-336	286	8	;	;	PUNCT
eurjchem-336	286	9	n	n	CCONJ
eurjchem-336	286	10	,	,	PUNCT
eurjchem-336	286	11	8.11	8.11	NUM
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eurjchem-336	286	13	.	.	PUNCT
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eurjchem-336	287	3	5e	5e	NOUN
eurjchem-336	287	4	):	):	PUNCT
eurjchem-336	287	5	ft‐ir	ft‐ir	NOUN
eurjchem-336	287	6	(	(	PUNCT
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eurjchem-336	287	8	,	,	PUNCT
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eurjchem-336	287	10	,	,	PUNCT
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eurjchem-336	287	12	):	):	PUNCT
eurjchem-336	287	13	1766	1766	NUM
eurjchem-336	287	14	.	.	PUNCT
eurjchem-336	288	1	1h	1h	NUM
eurjchem-336	288	2	nmr	nmr	NOUN
eurjchem-336	288	3	(	(	PUNCT
eurjchem-336	288	4	300	300	NUM
eurjchem-336	288	5	mhz	mhz	NOUN
eurjchem-336	288	6	,	,	PUNCT
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eurjchem-336	288	8	):	):	PUNCT
eurjchem-336	288	9	7.49	7.49	NUM
eurjchem-336	288	10	(	(	PUNCT
eurjchem-336	288	11	t	t	PROPN
eurjchem-336	288	12	,	,	PUNCT
eurjchem-336	288	13	1h	1h	NUM
eurjchem-336	288	14	,	,	PUNCT
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eurjchem-336	288	16	=	=	SYM
eurjchem-336	288	17	7.5	7.5	NUM
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eurjchem-336	288	19	,	,	PUNCT
eurjchem-336	288	20	ph‐h	ph‐h	PROPN
eurjchem-336	288	21	)	)	PUNCT
eurjchem-336	288	22	,	,	PUNCT
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eurjchem-336	288	24	(	(	PUNCT
eurjchem-336	288	25	t	t	PROPN
eurjchem-336	288	26	,	,	PUNCT
eurjchem-336	288	27	2h	2h	NUM
eurjchem-336	288	28	,	,	PUNCT
eurjchem-336	288	29	j	j	PROPN
eurjchem-336	288	30	=	=	SYM
eurjchem-336	288	31	7.5	7.5	NUM
eurjchem-336	288	32	hz	hz	ADJ
eurjchem-336	288	33	,	,	PUNCT
eurjchem-336	288	34	ph‐h	ph‐h	PROPN
eurjchem-336	288	35	)	)	PUNCT
eurjchem-336	288	36	,	,	PUNCT
eurjchem-336	288	37	7.83	7.83	NUM
eurjchem-336	288	38	(	(	PUNCT
eurjchem-336	288	39	d	d	PROPN
eurjchem-336	288	40	,	,	PUNCT
eurjchem-336	288	41	2h	2h	NUM
eurjchem-336	288	42	,	,	PUNCT
eurjchem-336	288	43	j	j	PROPN
eurjchem-336	288	44	=	=	SYM
eurjchem-336	288	45	7.8	7.8	NUM
eurjchem-336	288	46	hz	hz	NOUN
eurjchem-336	288	47	,	,	PUNCT
eurjchem-336	288	48	ph‐h	ph‐h	PROPN
eurjchem-336	288	49	)	)	PUNCT
eurjchem-336	288	50	,	,	PUNCT
eurjchem-336	288	51	7.88	7.88	NUM
eurjchem-336	288	52	(	(	PUNCT
eurjchem-336	288	53	d	d	PROPN
eurjchem-336	288	54	,	,	PUNCT
eurjchem-336	288	55	1h	1h	NUM
eurjchem-336	288	56	,	,	PUNCT
eurjchem-336	288	57	j	j	PROPN
eurjchem-336	288	58	=	=	SYM
eurjchem-336	288	59	2.1	2.1	NUM
eurjchem-336	288	60	hz	hz	NOUN
eurjchem-336	288	61	,	,	PUNCT
eurjchem-336	288	62	c7‐h	c7‐h	PROPN
eurjchem-336	288	63	)	)	PUNCT
eurjchem-336	288	64	,	,	PUNCT
eurjchem-336	288	65	8.29	8.29	NUM
eurjchem-336	288	66	(	(	PUNCT
eurjchem-336	288	67	d	d	PROPN
eurjchem-336	288	68	,	,	PUNCT
eurjchem-336	288	69	1h	1h	NUM
eurjchem-336	288	70	,	,	PUNCT
eurjchem-336	288	71	j	j	PROPN
eurjchem-336	288	72	=	=	SYM
eurjchem-336	288	73	2.1	2.1	NUM
eurjchem-336	288	74	hz	hz	ADJ
eurjchem-336	288	75	,	,	PUNCT
eurjchem-336	288	76	c9‐h	c9‐h	NOUN
eurjchem-336	288	77	)	)	PUNCT
eurjchem-336	288	78	,	,	PUNCT
eurjchem-336	288	79	8.71	8.71	NUM
eurjchem-336	288	80	(	(	PUNCT
eurjchem-336	288	81	s	s	PROPN
eurjchem-336	288	82	,	,	PUNCT
eurjchem-336	288	83	1h	1h	NUM
eurjchem-336	288	84	,	,	PUNCT
eurjchem-336	288	85	c3‐h	c3‐h	PROPN
eurjchem-336	288	86	)	)	PUNCT
eurjchem-336	288	87	.	.	PUNCT
eurjchem-336	289	1	13c	13c	NOUN
eurjchem-336	289	2	nmr	nmr	NOUN
eurjchem-336	289	3	(	(	PUNCT
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eurjchem-336	289	5	mhz	mhz	NOUN
eurjchem-336	289	6	,	,	PUNCT
eurjchem-336	289	7	dmso‐d6	dmso‐d6	NUM
eurjchem-336	289	8	):	):	PUNCT
eurjchem-336	289	9	107.8	107.8	NUM
eurjchem-336	289	10	,	,	PUNCT
eurjchem-336	289	11	116.1	116.1	NUM
eurjchem-336	289	12	,	,	PUNCT
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eurjchem-336	289	14	,	,	PUNCT
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eurjchem-336	289	16	,	,	PUNCT
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eurjchem-336	289	18	,	,	PUNCT
eurjchem-336	289	19	131.0	131.0	NUM
eurjchem-336	289	20	,	,	PUNCT
eurjchem-336	289	21	132.2	132.2	NUM
eurjchem-336	289	22	,	,	PUNCT
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eurjchem-336	289	24	,	,	PUNCT
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eurjchem-336	289	26	,	,	PUNCT
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eurjchem-336	289	28	,	,	PUNCT
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eurjchem-336	289	30	,	,	PUNCT
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eurjchem-336	289	32	,	,	PUNCT
eurjchem-336	289	33	152.9	152.9	NUM
eurjchem-336	289	34	,	,	PUNCT
eurjchem-336	289	35	161.2	161.2	NUM
eurjchem-336	289	36	.	.	PUNCT
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eurjchem-336	290	2	(	(	PUNCT
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eurjchem-336	290	4	,	,	PUNCT
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eurjchem-336	290	7	z	z	NOUN
eurjchem-336	290	8	):	):	PUNCT
eurjchem-336	290	9	418	418	NUM
eurjchem-336	290	10	(	(	PUNCT
eurjchem-336	290	11	m+	m+	NUM
eurjchem-336	290	12	)	)	PUNCT
eurjchem-336	290	13	.	.	PUNCT
eurjchem-336	291	1	anal	anal	PROPN
eurjchem-336	291	2	.	.	PUNCT
eurjchem-336	291	3	calcd	calcd	NOUN
eurjchem-336	291	4	.	.	PUNCT
eurjchem-336	292	1	for	for	ADP
eurjchem-336	292	2	c16h8n2o2br2	c16h8n2o2br2	NOUN
eurjchem-336	292	3	.	.	PUNCT
eurjchem-336	293	1	c	c	X
eurjchem-336	293	2	,	,	PUNCT
eurjchem-336	293	3	45.93	45.93	NUM
eurjchem-336	293	4	;	;	PUNCT
eurjchem-336	293	5	h	h	NOUN
eurjchem-336	293	6	,	,	PUNCT
eurjchem-336	293	7	1.91	1.91	NUM
eurjchem-336	293	8	;	;	PUNCT
eurjchem-336	293	9	n	n	CCONJ
eurjchem-336	293	10	,	,	PUNCT
eurjchem-336	293	11	6.69	6.69	NUM
eurjchem-336	293	12	.	.	PUNCT
eurjchem-336	293	13	found	find	VERB
eurjchem-336	293	14	:	:	PUNCT
eurjchem-336	294	1	c	c	X
eurjchem-336	294	2	,	,	PUNCT
eurjchem-336	294	3	46.12	46.12	NUM
eurjchem-336	294	4	;	;	PUNCT
eurjchem-336	294	5	h	h	NOUN
eurjchem-336	294	6	,	,	PUNCT
eurjchem-336	294	7	1.83	1.83	NUM
eurjchem-336	294	8	;	;	PUNCT
eurjchem-336	294	9	n	n	CCONJ
eurjchem-336	294	10	,	,	PUNCT
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eurjchem-336	294	12	%	%	NOUN
eurjchem-336	294	13	.	.	PUNCT
eurjchem-336	295	1	6‐bromo‐8‐chloro‐2‐phenylchromeno[4,3‐c]pyrazol‐4(2h)‐	6‐bromo‐8‐chloro‐2‐phenylchromeno[4,3‐c]pyrazol‐4(2h)‐	NUM
eurjchem-336	295	2	one	one	NUM
eurjchem-336	295	3	(	(	PUNCT
eurjchem-336	295	4	5f	5f	NOUN
eurjchem-336	295	5	):	):	PUNCT
eurjchem-336	295	6	ft‐ir	ft‐ir	NOUN
eurjchem-336	295	7	(	(	PUNCT
eurjchem-336	295	8	kbr	kbr	PROPN
eurjchem-336	295	9	,	,	PUNCT
eurjchem-336	295	10			PROPN
eurjchem-336	295	11	,	,	PUNCT
eurjchem-336	295	12	cm‐1	cm‐1	PROPN
eurjchem-336	295	13	):	):	PUNCT
eurjchem-336	295	14	1759	1759	NUM
eurjchem-336	295	15	.	.	PUNCT
eurjchem-336	296	1	1h	1h	NUM
eurjchem-336	296	2	nmr	nmr	NOUN
eurjchem-336	296	3	(	(	PUNCT
eurjchem-336	296	4	300	300	NUM
eurjchem-336	296	5	mhz	mhz	NOUN
eurjchem-336	296	6	,	,	PUNCT
eurjchem-336	296	7	dmso‐	dmso‐	NUM
eurjchem-336	296	8	d6	d6	NOUN
eurjchem-336	296	9	):	):	PUNCT
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eurjchem-336	296	11	(	(	PUNCT
eurjchem-336	296	12	t	t	PROPN
eurjchem-336	296	13	,	,	PUNCT
eurjchem-336	296	14	1h	1h	NUM
eurjchem-336	296	15	,	,	PUNCT
eurjchem-336	296	16	j	j	PROPN
eurjchem-336	296	17	=	=	SYM
eurjchem-336	296	18	7.5	7.5	NUM
eurjchem-336	296	19	hz	hz	ADJ
eurjchem-336	296	20	,	,	PUNCT
eurjchem-336	296	21	ph‐h	ph‐h	PROPN
eurjchem-336	296	22	)	)	PUNCT
eurjchem-336	296	23	,	,	PUNCT
eurjchem-336	296	24	7.59	7.59	NUM
eurjchem-336	296	25	(	(	PUNCT
eurjchem-336	296	26	t	t	PROPN
eurjchem-336	296	27	,	,	PUNCT
eurjchem-336	296	28	2h	2h	NUM
eurjchem-336	296	29	,	,	PUNCT
eurjchem-336	296	30	j	j	PROPN
eurjchem-336	296	31	=	=	SYM
eurjchem-336	296	32	7.5	7.5	NUM
eurjchem-336	296	33	hz	hz	ADJ
eurjchem-336	296	34	,	,	PUNCT
eurjchem-336	296	35	ph‐h	ph‐h	PROPN
eurjchem-336	296	36	)	)	PUNCT
eurjchem-336	296	37	,	,	PUNCT
eurjchem-336	296	38	7.75	7.75	NUM
eurjchem-336	296	39	(	(	PUNCT
eurjchem-336	296	40	d	d	PROPN
eurjchem-336	296	41	,	,	PUNCT
eurjchem-336	296	42	1h	1h	NUM
eurjchem-336	296	43	,	,	PUNCT
eurjchem-336	296	44	j	j	PROPN
eurjchem-336	296	45	=	=	SYM
eurjchem-336	296	46	2.4	2.4	NUM
eurjchem-336	296	47	hz	hz	NOUN
eurjchem-336	296	48	,	,	PUNCT
eurjchem-336	296	49	c7‐h	c7‐h	PROPN
eurjchem-336	296	50	)	)	PUNCT
eurjchem-336	296	51	,	,	PUNCT
eurjchem-336	296	52	7.85	7.85	NUM
eurjchem-336	296	53	(	(	PUNCT
eurjchem-336	296	54	d	d	PROPN
eurjchem-336	296	55	,	,	PUNCT
eurjchem-336	296	56	2h	2h	NUM
eurjchem-336	296	57	,	,	PUNCT
eurjchem-336	296	58	j	j	PROPN
eurjchem-336	296	59	=	=	SYM
eurjchem-336	296	60	7.5	7.5	NUM
eurjchem-336	296	61	hz	hz	ADJ
eurjchem-336	296	62	,	,	PUNCT
eurjchem-336	296	63	ph‐h	ph‐h	PROPN
eurjchem-336	296	64	)	)	PUNCT
eurjchem-336	296	65	,	,	PUNCT
eurjchem-336	296	66	8.15	8.15	NUM
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eurjchem-336	296	68	d	d	PROPN
eurjchem-336	296	69	,	,	PUNCT
eurjchem-336	296	70	1h	1h	NUM
eurjchem-336	296	71	,	,	PUNCT
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eurjchem-336	296	73	=	=	SYM
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eurjchem-336	296	75	,	,	PUNCT
eurjchem-336	296	76	c9‐h	c9‐h	NOUN
eurjchem-336	296	77	)	)	PUNCT
eurjchem-336	296	78	,	,	PUNCT
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eurjchem-336	296	81	s	s	PROPN
eurjchem-336	296	82	,	,	PUNCT
eurjchem-336	296	83	1h	1h	NUM
eurjchem-336	296	84	,	,	PUNCT
eurjchem-336	296	85	c3‐h	c3‐h	PROPN
eurjchem-336	296	86	)	)	PUNCT
eurjchem-336	296	87	.	.	PUNCT
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eurjchem-336	297	3	(	(	PUNCT
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eurjchem-336	297	6	,	,	PUNCT
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eurjchem-336	297	8	):	):	PUNCT
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eurjchem-336	297	10	,	,	PUNCT
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eurjchem-336	297	12	,	,	PUNCT
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eurjchem-336	297	14	,	,	PUNCT
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eurjchem-336	297	16	,	,	PUNCT
eurjchem-336	297	17	129.1	129.1	NUM
eurjchem-336	297	18	,	,	PUNCT
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eurjchem-336	297	20	,	,	PUNCT
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eurjchem-336	297	22	,	,	PUNCT
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eurjchem-336	297	24	,	,	PUNCT
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eurjchem-336	297	26	,	,	PUNCT
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eurjchem-336	297	28	,	,	PUNCT
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eurjchem-336	297	30	,	,	PUNCT
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eurjchem-336	297	32	,	,	PUNCT
eurjchem-336	297	33	151.0	151.0	NUM
eurjchem-336	297	34	,	,	PUNCT
eurjchem-336	297	35	157.5	157.5	NUM
eurjchem-336	297	36	.	.	PUNCT
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eurjchem-336	298	8	):	):	PUNCT
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eurjchem-336	298	10	(	(	PUNCT
eurjchem-336	298	11	m+	m+	NUM
eurjchem-336	298	12	)	)	PUNCT
eurjchem-336	298	13	.	.	PUNCT
eurjchem-336	299	1	anal	anal	PROPN
eurjchem-336	299	2	.	.	PUNCT
eurjchem-336	299	3	calcd	calcd	NOUN
eurjchem-336	299	4	.	.	PUNCT
eurjchem-336	300	1	for	for	ADP
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eurjchem-336	300	3	.	.	PUNCT
eurjchem-336	301	1	c	c	X
eurjchem-336	301	2	,	,	PUNCT
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eurjchem-336	301	4	;	;	PUNCT
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eurjchem-336	301	6	,	,	PUNCT
eurjchem-336	301	7	2.13	2.13	NUM
eurjchem-336	301	8	;	;	PUNCT
eurjchem-336	301	9	n	n	CCONJ
eurjchem-336	301	10	,	,	PUNCT
eurjchem-336	301	11	7.48	7.48	NUM
eurjchem-336	301	12	.	.	PUNCT
eurjchem-336	301	13	found	find	VERB
eurjchem-336	301	14	:	:	PUNCT
eurjchem-336	302	1	c	c	X
eurjchem-336	302	2	,	,	PUNCT
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eurjchem-336	302	4	;	;	PUNCT
eurjchem-336	303	1	h	h	NOUN
eurjchem-336	303	2	,	,	PUNCT
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eurjchem-336	303	4	;	;	PUNCT
eurjchem-336	303	5	n	n	CCONJ
eurjchem-336	303	6	,	,	PUNCT
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eurjchem-336	303	8	%	%	NOUN
eurjchem-336	303	9	.	.	PUNCT
eurjchem-336	304	1	6‐bromo‐8‐methyl‐2‐phenylchromeno[4,3‐c]pyrazol‐4(2h)‐	6‐bromo‐8‐methyl‐2‐phenylchromeno[4,3‐c]pyrazol‐4(2h)‐	VERB
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eurjchem-336	304	4	5	5	NUM
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eurjchem-336	304	6	):	):	PUNCT
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eurjchem-336	304	8	(	(	PUNCT
eurjchem-336	304	9	kbr	kbr	PROPN
eurjchem-336	304	10	,	,	PUNCT
eurjchem-336	304	11			PROPN
eurjchem-336	304	12	,	,	PUNCT
eurjchem-336	304	13	cm‐1	cm‐1	PROPN
eurjchem-336	304	14	):	):	PUNCT
eurjchem-336	304	15	1741	1741	NUM
eurjchem-336	304	16	.	.	PUNCT
eurjchem-336	305	1	1h	1h	NUM
eurjchem-336	305	2	nmr	nmr	NOUN
eurjchem-336	305	3	(	(	PUNCT
eurjchem-336	305	4	300	300	NUM
eurjchem-336	305	5	mhz	mhz	NOUN
eurjchem-336	305	6	,	,	PUNCT
eurjchem-336	305	7	dmso‐	dmso‐	NUM
eurjchem-336	305	8	d6	d6	NOUN
eurjchem-336	305	9	):	):	PUNCT
eurjchem-336	305	10	2.44	2.44	NUM
eurjchem-336	305	11	(	(	PUNCT
eurjchem-336	305	12	s	s	PROPN
eurjchem-336	305	13	,	,	PUNCT
eurjchem-336	305	14	3h	3h	NUM
eurjchem-336	305	15	,	,	PUNCT
eurjchem-336	305	16	ch3	ch3	PROPN
eurjchem-336	305	17	)	)	PUNCT
eurjchem-336	305	18	,	,	PUNCT
eurjchem-336	305	19	7.46	7.46	NUM
eurjchem-336	305	20	(	(	PUNCT
eurjchem-336	305	21	t	t	PROPN
eurjchem-336	305	22	,	,	PUNCT
eurjchem-336	305	23	1h	1h	NUM
eurjchem-336	305	24	,	,	PUNCT
eurjchem-336	305	25	j	j	PROPN
eurjchem-336	305	26	=	=	SYM
eurjchem-336	305	27	7.2	7.2	NUM
eurjchem-336	305	28	hz	hz	NOUN
eurjchem-336	305	29	,	,	PUNCT
eurjchem-336	305	30	ph‐h	ph‐h	PROPN
eurjchem-336	305	31	)	)	PUNCT
eurjchem-336	305	32	,	,	PUNCT
eurjchem-336	305	33	7.54‐	7.54‐	NUM
eurjchem-336	305	34	7.59	7.59	NUM
eurjchem-336	305	35	(	(	PUNCT
eurjchem-336	305	36	m	m	PROPN
eurjchem-336	305	37	,	,	PUNCT
eurjchem-336	305	38	3h	3h	NUM
eurjchem-336	305	39	,	,	PUNCT
eurjchem-336	305	40	c7‐h	c7‐h	PROPN
eurjchem-336	305	41	&	&	CCONJ
eurjchem-336	305	42	ph‐h	ph‐h	PROPN
eurjchem-336	305	43	)	)	PUNCT
eurjchem-336	305	44	,	,	PUNCT
eurjchem-336	305	45	7.84	7.84	NUM
eurjchem-336	305	46	(	(	PUNCT
eurjchem-336	305	47	d	d	PROPN
eurjchem-336	305	48	,	,	PUNCT
eurjchem-336	305	49	2h	2h	NUM
eurjchem-336	305	50	,	,	PUNCT
eurjchem-336	305	51	j	j	PROPN
eurjchem-336	306	1	=	=	SYM
eurjchem-336	306	2	7.5	7.5	NUM
eurjchem-336	306	3	hz	hz	ADJ
eurjchem-336	306	4	,	,	PUNCT
eurjchem-336	306	5	ph‐h	ph‐h	PROPN
eurjchem-336	306	6	)	)	PUNCT
eurjchem-336	306	7	,	,	PUNCT
eurjchem-336	306	8	7.95	7.95	NUM
eurjchem-336	306	9	(	(	PUNCT
eurjchem-336	306	10	d	d	PROPN
eurjchem-336	306	11	,	,	PUNCT
eurjchem-336	306	12	1h	1h	NUM
eurjchem-336	306	13	,	,	PUNCT
eurjchem-336	306	14	j	j	PROPN
eurjchem-336	306	15	=	=	PROPN
eurjchem-336	306	16	1.2	1.2	NUM
eurjchem-336	306	17	hz	hz	ADJ
eurjchem-336	306	18	,	,	PUNCT
eurjchem-336	306	19	c9‐h	c9‐h	NOUN
eurjchem-336	306	20	)	)	PUNCT
eurjchem-336	306	21	,	,	PUNCT
eurjchem-336	306	22	8.69	8.69	NUM
eurjchem-336	306	23	(	(	PUNCT
eurjchem-336	306	24	s	s	PROPN
eurjchem-336	306	25	,	,	PUNCT
eurjchem-336	306	26	1h	1h	NUM
eurjchem-336	306	27	,	,	PUNCT
eurjchem-336	306	28	c3‐h	c3‐h	PROPN
eurjchem-336	306	29	)	)	PUNCT
eurjchem-336	306	30	.	.	PUNCT
eurjchem-336	307	1	13c	13c	NOUN
eurjchem-336	307	2	nmr	nmr	NOUN
eurjchem-336	307	3	(	(	PUNCT
eurjchem-336	307	4	75	75	NUM
eurjchem-336	307	5	mhz	mhz	NOUN
eurjchem-336	307	6	,	,	PUNCT
eurjchem-336	307	7	dmso‐	dmso‐	NUM
eurjchem-336	307	8	d6	d6	NOUN
eurjchem-336	307	9	):	):	PUNCT
eurjchem-336	307	10	25.1	25.1	NUM
eurjchem-336	307	11	,	,	PUNCT
eurjchem-336	307	12	110.9	110.9	NUM
eurjchem-336	307	13	,	,	PUNCT
eurjchem-336	307	14	117.4	117.4	NUM
eurjchem-336	307	15	,	,	PUNCT
eurjchem-336	307	16	122.1	122.1	NUM
eurjchem-336	307	17	,	,	PUNCT
eurjchem-336	307	18	127.9	127.9	NUM
eurjchem-336	307	19	,	,	PUNCT
eurjchem-336	307	20	130.3	130.3	NUM
eurjchem-336	307	21	,	,	PUNCT
eurjchem-336	307	22	131.2	131.2	NUM
eurjchem-336	307	23	,	,	PUNCT
eurjchem-336	307	24	131.7	131.7	NUM
eurjchem-336	307	25	,	,	PUNCT
eurjchem-336	307	26	132.0	132.0	NUM
eurjchem-336	307	27	,	,	PUNCT
eurjchem-336	307	28	134.7	134.7	NUM
eurjchem-336	307	29	,	,	PUNCT
eurjchem-336	307	30	139.9	139.9	NUM
eurjchem-336	307	31	,	,	PUNCT
eurjchem-336	307	32	140.8	140.8	NUM
eurjchem-336	307	33	,	,	PUNCT
eurjchem-336	307	34	148.4	148.4	NUM
eurjchem-336	307	35	,	,	PUNCT
eurjchem-336	307	36	150.4	150.4	NUM
eurjchem-336	307	37	,	,	PUNCT
eurjchem-336	307	38	157.1	157.1	NUM
eurjchem-336	307	39	.	.	PUNCT
eurjchem-336	308	1	ms	ms	NOUN
eurjchem-336	308	2	(	(	PUNCT
eurjchem-336	308	3	ei	ei	PROPN
eurjchem-336	308	4	,	,	PUNCT
eurjchem-336	308	5	m	m	PROPN
eurjchem-336	308	6	/	/	SYM
eurjchem-336	308	7	z	z	NOUN
eurjchem-336	308	8	):	):	PUNCT
eurjchem-336	308	9	354	354	NUM
eurjchem-336	308	10	(	(	PUNCT
eurjchem-336	308	11	m+	m+	NUM
eurjchem-336	308	12	)	)	PUNCT
eurjchem-336	308	13	.	.	PUNCT
eurjchem-336	309	1	anal	anal	PROPN
eurjchem-336	309	2	.	.	PUNCT
eurjchem-336	309	3	calcd	calcd	NOUN
eurjchem-336	309	4	.	.	PUNCT
eurjchem-336	310	1	for	for	ADP
eurjchem-336	310	2	c17h11n2o2br	c17h11n2o2br	PROPN
eurjchem-336	310	3	.	.	PUNCT
eurjchem-336	311	1	c	c	X
eurjchem-336	311	2	,	,	PUNCT
eurjchem-336	311	3	57.62	57.62	NUM
eurjchem-336	311	4	;	;	PUNCT
eurjchem-336	311	5	h	h	NOUN
eurjchem-336	311	6	,	,	PUNCT
eurjchem-336	311	7	3.10	3.10	NUM
eurjchem-336	311	8	;	;	PUNCT
eurjchem-336	311	9	n	n	CCONJ
eurjchem-336	311	10	,	,	PUNCT
eurjchem-336	311	11	7.90	7.90	NUM
eurjchem-336	311	12	.	.	PUNCT
eurjchem-336	311	13	found	find	VERB
eurjchem-336	311	14	:	:	PUNCT
eurjchem-336	312	1	c	c	X
eurjchem-336	312	2	,	,	PUNCT
eurjchem-336	312	3	57.41	57.41	NUM
eurjchem-336	312	4	;	;	PUNCT
eurjchem-336	312	5	h	h	NOUN
eurjchem-336	312	6	,	,	PUNCT
eurjchem-336	312	7	2.93	2.93	NUM
eurjchem-336	312	8	;	;	PUNCT
eurjchem-336	312	9	n	n	CCONJ
eurjchem-336	312	10	,	,	PUNCT
eurjchem-336	312	11	7.61	7.61	NUM
eurjchem-336	312	12	%	%	NOUN
eurjchem-336	312	13	.	.	PUNCT
eurjchem-336	313	1	2.2.6	2.2.6	X
eurjchem-336	313	2	.	.	PUNCT
eurjchem-336	313	3	general	general	ADJ
eurjchem-336	313	4	procedure	procedure	NOUN
eurjchem-336	313	5	for	for	ADP
eurjchem-336	313	6	the	the	DET
eurjchem-336	313	7	preparation	preparation	NOUN
eurjchem-336	313	8	of	of	ADP
eurjchem-336	313	9	substituted	substitute	VERB
eurjchem-336	313	10	of	of	ADP
eurjchem-336	313	11	2‐arylpyrazolo	2‐arylpyrazolo	NOUN
eurjchem-336	313	12	[	[	X
eurjchem-336	313	13	4	4	NUM
eurjchem-336	313	14	,	,	PUNCT
eurjchem-336	313	15	3‐c	3‐c	NUM
eurjchem-336	313	16	]	]	PUNCT
eurjchem-336	313	17	coumarin	coumarin	NOUN
eurjchem-336	313	18	derivatives	derivative	NOUN
eurjchem-336	313	19	(	(	PUNCT
eurjchem-336	313	20	6a‐c	6a‐c	NOUN
eurjchem-336	313	21	)	)	PUNCT
eurjchem-336	313	22	to	to	ADP
eurjchem-336	313	23	a	a	DET
eurjchem-336	313	24	solution	solution	NOUN
eurjchem-336	313	25	of	of	ADP
eurjchem-336	313	26	3‐(2‐hydroxyaryl)‐1‐phenyl‐1h‐pyrazole‐	3‐(2‐hydroxyaryl)‐1‐phenyl‐1h‐pyrazole‐	NUM
eurjchem-336	313	27	4‐carbaldehydes	4‐carbaldehyde	NOUN
eurjchem-336	313	28	(	(	PUNCT
eurjchem-336	313	29	3a‐c	3a‐c	NUM
eurjchem-336	313	30	)	)	PUNCT
eurjchem-336	313	31	(	(	PUNCT
eurjchem-336	313	32	1	1	NUM
eurjchem-336	313	33	mmol	mmol	NOUN
eurjchem-336	313	34	)	)	PUNCT
eurjchem-336	313	35	or	or	CCONJ
eurjchem-336	313	36	3‐(2‐(allyloxyaryl)‐1‐	3‐(2‐(allyloxyaryl)‐1‐	NUM
eurjchem-336	313	37	phenyl‐1h‐pyrazole‐4‐carbaldehydes	phenyl‐1h‐pyrazole‐4‐carbaldehyde	NOUN
eurjchem-336	313	38	(	(	PUNCT
eurjchem-336	313	39	4a‐c	4a‐c	NOUN
eurjchem-336	313	40	)	)	PUNCT
eurjchem-336	313	41	(	(	PUNCT
eurjchem-336	313	42	1	1	NUM
eurjchem-336	313	43	mmol	mmol	NOUN
eurjchem-336	313	44	)	)	PUNCT
eurjchem-336	313	45	in	in	ADP
eurjchem-336	313	46	dmso	dmso	NOUN
eurjchem-336	313	47	(	(	PUNCT
eurjchem-336	313	48	20	20	NUM
eurjchem-336	313	49	ml	ml	NOUN
eurjchem-336	313	50	)	)	PUNCT
eurjchem-336	313	51	,	,	PUNCT
eurjchem-336	313	52	iodine	iodine	NOUN
eurjchem-336	313	53	(	(	PUNCT
eurjchem-336	313	54	1.2	1.2	NUM
eurjchem-336	313	55	equivalent	equivalent	NOUN
eurjchem-336	313	56	)	)	PUNCT
eurjchem-336	313	57	and	and	CCONJ
eurjchem-336	313	58	4‐5	4‐5	NOUN
eurjchem-336	313	59	drops	drop	NOUN
eurjchem-336	313	60	of	of	ADP
eurjchem-336	313	61	concentrated	concentrated	ADJ
eurjchem-336	313	62	h2so4	h2so4	PROPN
eurjchem-336	313	63	was	be	AUX
eurjchem-336	313	64	added	add	VERB
eurjchem-336	313	65	.	.	PUNCT
eurjchem-336	314	1	then	then	ADV
eurjchem-336	314	2	the	the	DET
eurjchem-336	314	3	reaction	reaction	NOUN
eurjchem-336	314	4	mixture	mixture	NOUN
eurjchem-336	314	5	was	be	AUX
eurjchem-336	314	6	heated	heat	VERB
eurjchem-336	314	7	at	at	ADP
eurjchem-336	314	8	120	120	NUM
eurjchem-336	314	9	oc	oc	NOUN
eurjchem-336	314	10	.	.	PUNCT
eurjchem-336	315	1	after	after	ADP
eurjchem-336	315	2	the	the	DET
eurjchem-336	315	3	completion	completion	NOUN
eurjchem-336	315	4	of	of	ADP
eurjchem-336	315	5	the	the	DET
eurjchem-336	315	6	reaction	reaction	NOUN
eurjchem-336	315	7	(	(	PUNCT
eurjchem-336	315	8	checked	check	VERB
eurjchem-336	315	9	by	by	ADP
eurjchem-336	315	10	tlc	tlc	PROPN
eurjchem-336	315	11	)	)	PUNCT
eurjchem-336	315	12	,	,	PUNCT
eurjchem-336	315	13	the	the	DET
eurjchem-336	315	14	contents	content	NOUN
eurjchem-336	315	15	were	be	AUX
eurjchem-336	315	16	cooled	cool	VERB
eurjchem-336	315	17	to	to	ADP
eurjchem-336	315	18	room	room	NOUN
eurjchem-336	315	19	temperature	temperature	NOUN
eurjchem-336	315	20	and	and	CCONJ
eurjchem-336	315	21	poured	pour	VERB
eurjchem-336	315	22	into	into	ADP
eurjchem-336	315	23	ice‐	ice‐	PROPN
eurjchem-336	315	24	cooled	cooled	ADJ
eurjchem-336	315	25	water	water	NOUN
eurjchem-336	315	26	.	.	PUNCT
eurjchem-336	316	1	the	the	DET
eurjchem-336	316	2	separated	separate	VERB
eurjchem-336	316	3	solid	solid	ADJ
eurjchem-336	316	4	was	be	AUX
eurjchem-336	316	5	filtered	filter	VERB
eurjchem-336	316	6	and	and	CCONJ
eurjchem-336	316	7	washed	wash	VERB
eurjchem-336	316	8	with	with	ADP
eurjchem-336	316	9	cooled	cooled	ADJ
eurjchem-336	316	10	dilute	dilute	NOUN
eurjchem-336	316	11	sodium	sodium	NOUN
eurjchem-336	316	12	thiosulphate	thiosulphate	NOUN
eurjchem-336	316	13	solution	solution	NOUN
eurjchem-336	316	14	.	.	PUNCT
eurjchem-336	317	1	finally	finally	ADV
eurjchem-336	317	2	the	the	DET
eurjchem-336	317	3	obtained	obtain	VERB
eurjchem-336	317	4	product	product	NOUN
eurjchem-336	317	5	was	be	AUX
eurjchem-336	317	6	crystallized	crystallize	VERB
eurjchem-336	317	7	from	from	ADP
eurjchem-336	317	8	dmf	dmf	PROPN
eurjchem-336	317	9	to	to	PART
eurjchem-336	317	10	give	give	VERB
eurjchem-336	317	11	product	product	NOUN
eurjchem-336	317	12	6a‐c	6a‐c	NOUN
eurjchem-336	317	13	.	.	PUNCT
eurjchem-336	318	1	8‐chloro‐6‐iodo‐2‐phenylchromeno[4,3‐c]pyrazol‐4(2h)‐one	8‐chloro‐6‐iodo‐2‐phenylchromeno[4,3‐c]pyrazol‐4(2h)‐one	NUM
eurjchem-336	318	2	(	(	PUNCT
eurjchem-336	318	3	6a	6a	NOUN
eurjchem-336	318	4	):	):	PUNCT
eurjchem-336	318	5	ft‐ir	ft‐ir	NOUN
eurjchem-336	318	6	(	(	PUNCT
eurjchem-336	318	7	kbr	kbr	PROPN
eurjchem-336	318	8	,	,	PUNCT
eurjchem-336	318	9			PROPN
eurjchem-336	318	10	,	,	PUNCT
eurjchem-336	318	11	cm‐1	cm‐1	PROPN
eurjchem-336	318	12	):	):	PUNCT
eurjchem-336	318	13	1745	1745	NUM
eurjchem-336	318	14	.	.	PUNCT
eurjchem-336	319	1	1h	1h	NUM
eurjchem-336	319	2	nmr	nmr	NOUN
eurjchem-336	319	3	(	(	PUNCT
eurjchem-336	319	4	300	300	NUM
eurjchem-336	319	5	mhz	mhz	NOUN
eurjchem-336	319	6	,	,	PUNCT
eurjchem-336	319	7	dmso‐d6	dmso‐d6	NUM
eurjchem-336	319	8	):	):	PUNCT
eurjchem-336	319	9	7.48	7.48	NUM
eurjchem-336	319	10	(	(	PUNCT
eurjchem-336	319	11	t	t	PROPN
eurjchem-336	319	12	,	,	PUNCT
eurjchem-336	319	13	1h	1h	NUM
eurjchem-336	319	14	,	,	PUNCT
eurjchem-336	319	15	j	j	PROPN
eurjchem-336	319	16	=	=	SYM
eurjchem-336	319	17	7.5	7.5	NUM
eurjchem-336	319	18	hz	hz	ADJ
eurjchem-336	319	19	,	,	PUNCT
eurjchem-336	319	20	ph‐h	ph‐h	PROPN
eurjchem-336	319	21	)	)	PUNCT
eurjchem-336	319	22	,	,	PUNCT
eurjchem-336	319	23	7.57	7.57	NUM
eurjchem-336	319	24	(	(	PUNCT
eurjchem-336	319	25	t	t	PROPN
eurjchem-336	319	26	,	,	PUNCT
eurjchem-336	319	27	2h	2h	NUM
eurjchem-336	319	28	,	,	PUNCT
eurjchem-336	319	29	j	j	PROPN
eurjchem-336	319	30	=	=	SYM
eurjchem-336	319	31	7.5	7.5	NUM
eurjchem-336	319	32	hz	hz	ADJ
eurjchem-336	319	33	,	,	PUNCT
eurjchem-336	319	34	ph‐h	ph‐h	PROPN
eurjchem-336	319	35	)	)	PUNCT
eurjchem-336	319	36	,	,	PUNCT
eurjchem-336	319	37	7.83	7.83	NUM
eurjchem-336	319	38	(	(	PUNCT
eurjchem-336	319	39	d	d	PROPN
eurjchem-336	319	40	,	,	PUNCT
eurjchem-336	319	41	2h	2h	NUM
eurjchem-336	319	42	,	,	PUNCT
eurjchem-336	319	43	j	j	PROPN
eurjchem-336	319	44	=	=	PROPN
eurjchem-336	319	45	8.4	8.4	NUM
eurjchem-336	319	46	hz	hz	NOUN
eurjchem-336	319	47	,	,	PUNCT
eurjchem-336	319	48	ph‐h	ph‐h	PROPN
eurjchem-336	319	49	)	)	PUNCT
eurjchem-336	319	50	,	,	PUNCT
eurjchem-336	319	51	7.94	7.94	NUM
eurjchem-336	319	52	(	(	PUNCT
eurjchem-336	319	53	d	d	PROPN
eurjchem-336	319	54	,	,	PUNCT
eurjchem-336	319	55	1h	1h	NUM
eurjchem-336	319	56	,	,	PUNCT
eurjchem-336	319	57	j	j	PROPN
eurjchem-336	319	58	=	=	SYM
eurjchem-336	319	59	2.4	2.4	NUM
eurjchem-336	319	60	hz	hz	NOUN
eurjchem-336	319	61	,	,	PUNCT
eurjchem-336	319	62	c7‐h	c7‐h	PROPN
eurjchem-336	319	63	)	)	PUNCT
eurjchem-336	319	64	,	,	PUNCT
eurjchem-336	319	65	8.16	8.16	NUM
eurjchem-336	319	66	(	(	PUNCT
eurjchem-336	319	67	d	d	PROPN
eurjchem-336	319	68	,	,	PUNCT
eurjchem-336	319	69	1h	1h	NUM
eurjchem-336	319	70	,	,	PUNCT
eurjchem-336	319	71	j	j	PROPN
eurjchem-336	319	72	=	=	SYM
eurjchem-336	319	73	2.4	2.4	NUM
eurjchem-336	319	74	hz	hz	ADJ
eurjchem-336	319	75	,	,	PUNCT
eurjchem-336	319	76	c9‐h	c9‐h	NOUN
eurjchem-336	319	77	)	)	PUNCT
eurjchem-336	319	78	,	,	PUNCT
eurjchem-336	319	79	8.71	8.71	NUM
eurjchem-336	319	80	(	(	PUNCT
eurjchem-336	319	81	s	s	PROPN
eurjchem-336	319	82	,	,	PUNCT
eurjchem-336	319	83	1h	1h	NUM
eurjchem-336	319	84	,	,	PUNCT
eurjchem-336	319	85	c3‐h	c3‐h	PROPN
eurjchem-336	319	86	)	)	PUNCT
eurjchem-336	319	87	.	.	PUNCT
eurjchem-336	320	1	13c	13c	NOUN
eurjchem-336	320	2	nmr	nmr	NOUN
eurjchem-336	320	3	(	(	PUNCT
eurjchem-336	320	4	75	75	NUM
eurjchem-336	320	5	mhz	mhz	NOUN
eurjchem-336	320	6	,	,	PUNCT
eurjchem-336	320	7	dmso‐d6	dmso‐d6	NUM
eurjchem-336	320	8	):	):	PUNCT
eurjchem-336	320	9	87.3	87.3	NUM
eurjchem-336	320	10	,	,	PUNCT
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eurjchem-336	320	12	,	,	PUNCT
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eurjchem-336	320	14	,	,	PUNCT
eurjchem-336	320	15	119.9	119.9	NUM
eurjchem-336	320	16	,	,	PUNCT
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eurjchem-336	320	18	,	,	PUNCT
eurjchem-336	320	19	128.5	128.5	NUM
eurjchem-336	320	20	,	,	PUNCT
eurjchem-336	320	21	129.3	129.3	NUM
eurjchem-336	320	22	,	,	PUNCT
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eurjchem-336	320	30	,	,	PUNCT
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eurjchem-336	321	10	(	(	PUNCT
eurjchem-336	321	11	m+	m+	NUM
eurjchem-336	321	12	)	)	PUNCT
eurjchem-336	321	13	.	.	PUNCT
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eurjchem-336	322	2	.	.	PUNCT
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eurjchem-336	322	4	.	.	PUNCT
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eurjchem-336	323	5	,	,	PUNCT
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eurjchem-336	323	7	;	;	PUNCT
eurjchem-336	323	8	h	h	NOUN
eurjchem-336	323	9	,	,	PUNCT
eurjchem-336	323	10	1.89	1.89	NUM
eurjchem-336	323	11	;	;	PUNCT
eurjchem-336	323	12	n	n	CCONJ
eurjchem-336	323	13	,	,	PUNCT
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eurjchem-336	323	17	:	:	PUNCT
eurjchem-336	324	1	c	c	X
eurjchem-336	324	2	,	,	PUNCT
eurjchem-336	324	3	45.61	45.61	NUM
eurjchem-336	324	4	;	;	PUNCT
eurjchem-336	324	5	h	h	NOUN
eurjchem-336	324	6	,	,	PUNCT
eurjchem-336	324	7	2.01	2.01	NUM
eurjchem-336	324	8	;	;	PUNCT
eurjchem-336	324	9	n	n	CCONJ
eurjchem-336	324	10	,	,	PUNCT
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eurjchem-336	324	13	.	.	PUNCT
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eurjchem-336	325	3	6b	6b	NOUN
eurjchem-336	325	4	):	):	PUNCT
eurjchem-336	325	5	ft‐ir	ft‐ir	NOUN
eurjchem-336	325	6	(	(	PUNCT
eurjchem-336	325	7	kbr	kbr	PROPN
eurjchem-336	325	8	,	,	PUNCT
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eurjchem-336	325	10	,	,	PUNCT
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eurjchem-336	325	12	):	):	PUNCT
eurjchem-336	325	13	1743	1743	NUM
eurjchem-336	325	14	.	.	PUNCT
eurjchem-336	326	1	1h	1h	NUM
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eurjchem-336	326	3	(	(	PUNCT
eurjchem-336	326	4	300	300	NUM
eurjchem-336	326	5	mhz	mhz	NOUN
eurjchem-336	326	6	,	,	PUNCT
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eurjchem-336	326	8	):	):	PUNCT
eurjchem-336	326	9	7.47	7.47	NUM
eurjchem-336	326	10	(	(	PUNCT
eurjchem-336	326	11	t	t	PROPN
eurjchem-336	326	12	,	,	PUNCT
eurjchem-336	326	13	1h	1h	NUM
eurjchem-336	326	14	,	,	PUNCT
eurjchem-336	326	15	j	j	PROPN
eurjchem-336	326	16	=	=	SYM
eurjchem-336	326	17	7.8	7.8	NUM
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eurjchem-336	326	19	,	,	PUNCT
eurjchem-336	326	20	ph‐h	ph‐h	PROPN
eurjchem-336	326	21	)	)	PUNCT
eurjchem-336	326	22	,	,	PUNCT
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eurjchem-336	326	25	t	t	PROPN
eurjchem-336	326	26	,	,	PUNCT
eurjchem-336	326	27	2h	2h	NUM
eurjchem-336	326	28	,	,	PUNCT
eurjchem-336	326	29	j	j	PROPN
eurjchem-336	326	30	=	=	SYM
eurjchem-336	326	31	7.8	7.8	NUM
eurjchem-336	326	32	hz	hz	NOUN
eurjchem-336	326	33	,	,	PUNCT
eurjchem-336	326	34	ph‐h	ph‐h	PROPN
eurjchem-336	326	35	)	)	PUNCT
eurjchem-336	326	36	,	,	PUNCT
eurjchem-336	326	37	7.83	7.83	NUM
eurjchem-336	326	38	(	(	PUNCT
eurjchem-336	326	39	d	d	PROPN
eurjchem-336	326	40	,	,	PUNCT
eurjchem-336	326	41	2h	2h	NUM
eurjchem-336	326	42	,	,	PUNCT
eurjchem-336	326	43	j	j	PROPN
eurjchem-336	326	44	=	=	SYM
eurjchem-336	326	45	7.8	7.8	NUM
eurjchem-336	326	46	hz	hz	NOUN
eurjchem-336	326	47	,	,	PUNCT
eurjchem-336	326	48	ph‐h	ph‐h	PROPN
eurjchem-336	326	49	)	)	PUNCT
eurjchem-336	326	50	,	,	PUNCT
eurjchem-336	326	51	8.08	8.08	NUM
eurjchem-336	326	52	(	(	PUNCT
eurjchem-336	326	53	d	d	PROPN
eurjchem-336	326	54	,	,	PUNCT
eurjchem-336	326	55	1h	1h	NUM
eurjchem-336	326	56	,	,	PUNCT
eurjchem-336	326	57	j	j	PROPN
eurjchem-336	326	58	=	=	SYM
eurjchem-336	326	59	2.4	2.4	NUM
eurjchem-336	326	60	hz	hz	NOUN
eurjchem-336	326	61	,	,	PUNCT
eurjchem-336	326	62	c7‐h	c7‐h	PROPN
eurjchem-336	326	63	)	)	PUNCT
eurjchem-336	326	64	,	,	PUNCT
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eurjchem-336	326	66	(	(	PUNCT
eurjchem-336	326	67	d	d	PROPN
eurjchem-336	326	68	,	,	PUNCT
eurjchem-336	326	69	1h	1h	NUM
eurjchem-336	326	70	,	,	PUNCT
eurjchem-336	326	71	j	j	PROPN
eurjchem-336	326	72	=	=	SYM
eurjchem-336	326	73	2.1	2.1	NUM
eurjchem-336	326	74	hz	hz	ADJ
eurjchem-336	326	75	,	,	PUNCT
eurjchem-336	326	76	c9‐h	c9‐h	NOUN
eurjchem-336	326	77	)	)	PUNCT
eurjchem-336	326	78	,	,	PUNCT
eurjchem-336	326	79	8.70	8.70	NUM
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eurjchem-336	326	81	s	s	PROPN
eurjchem-336	326	82	,	,	PUNCT
eurjchem-336	326	83	1h	1h	NUM
eurjchem-336	326	84	,	,	PUNCT
eurjchem-336	326	85	c3‐h	c3‐h	PROPN
eurjchem-336	326	86	)	)	PUNCT
eurjchem-336	326	87	.	.	PUNCT
eurjchem-336	327	1	13c	13c	NOUN
eurjchem-336	327	2	nmr	nmr	NOUN
eurjchem-336	327	3	(	(	PUNCT
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eurjchem-336	327	5	mhz	mhz	NOUN
eurjchem-336	327	6	,	,	PUNCT
eurjchem-336	327	7	dmso‐d6	dmso‐d6	NUM
eurjchem-336	327	8	):	):	PUNCT
eurjchem-336	327	9	87.9	87.9	NUM
eurjchem-336	327	10	,	,	PUNCT
eurjchem-336	327	11	108.2	108.2	NUM
eurjchem-336	327	12	,	,	PUNCT
eurjchem-336	327	13	115.4	115.4	NUM
eurjchem-336	327	14	,	,	PUNCT
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eurjchem-336	327	16	,	,	PUNCT
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eurjchem-336	327	18	,	,	PUNCT
eurjchem-336	327	19	124.2	124.2	NUM
eurjchem-336	327	20	,	,	PUNCT
eurjchem-336	327	21	129.7	129.7	NUM
eurjchem-336	327	22	,	,	PUNCT
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eurjchem-336	327	24	,	,	PUNCT
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eurjchem-336	327	26	,	,	PUNCT
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eurjchem-336	327	28	,	,	PUNCT
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eurjchem-336	327	30	,	,	PUNCT
eurjchem-336	327	31	148.1	148.1	NUM
eurjchem-336	327	32	,	,	PUNCT
eurjchem-336	327	33	151.8	151.8	NUM
eurjchem-336	327	34	,	,	PUNCT
eurjchem-336	327	35	156.3	156.3	NUM
eurjchem-336	327	36	.	.	PUNCT
eurjchem-336	328	1	ms	ms	NOUN
eurjchem-336	328	2	(	(	PUNCT
eurjchem-336	328	3	ei	ei	PROPN
eurjchem-336	328	4	,	,	PUNCT
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eurjchem-336	328	7	z	z	NOUN
eurjchem-336	328	8	):	):	PUNCT
eurjchem-336	328	9	466	466	NUM
eurjchem-336	328	10	(	(	PUNCT
eurjchem-336	328	11	m+	m+	NUM
eurjchem-336	328	12	)	)	PUNCT
eurjchem-336	328	13	.	.	PUNCT
eurjchem-336	329	1	anal	anal	PROPN
eurjchem-336	329	2	.	.	PUNCT
eurjchem-336	329	3	calcd	calcd	NOUN
eurjchem-336	329	4	.	.	PUNCT
eurjchem-336	330	1	for	for	ADP
eurjchem-336	330	2	c16h8n2o2bri	c16h8n2o2bri	PROPN
eurjchem-336	330	3	.	.	PROPN
eurjchem-336	330	4	c	c	X
eurjchem-336	330	5	,	,	PUNCT
eurjchem-336	330	6	41.20	41.20	NUM
eurjchem-336	330	7	;	;	PUNCT
eurjchem-336	330	8	h	h	NOUN
eurjchem-336	330	9	,	,	PUNCT
eurjchem-336	330	10	1.71	1.71	NUM
eurjchem-336	330	11	;	;	PUNCT
eurjchem-336	330	12	n	n	CCONJ
eurjchem-336	330	13	,	,	PUNCT
eurjchem-336	330	14	6.00	6.00	NUM
eurjchem-336	330	15	.	.	PUNCT
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eurjchem-336	330	17	:	:	PUNCT
eurjchem-336	331	1	c	c	X
eurjchem-336	331	2	,	,	PUNCT
eurjchem-336	331	3	41.51	41.51	NUM
eurjchem-336	331	4	;	;	PUNCT
eurjchem-336	331	5	h	h	NOUN
eurjchem-336	331	6	,	,	PUNCT
eurjchem-336	331	7	1.87	1.87	NUM
eurjchem-336	331	8	;	;	PUNCT
eurjchem-336	331	9	n	n	CCONJ
eurjchem-336	331	10	,	,	PUNCT
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eurjchem-336	331	12	%	%	NOUN
eurjchem-336	331	13	.	.	PUNCT
eurjchem-336	332	1	6‐chloro‐8‐iodo‐2‐phenylchromeno[4,3‐c]pyrazol‐4(2h)‐one	6‐chloro‐8‐iodo‐2‐phenylchromeno[4,3‐c]pyrazol‐4(2h)‐one	NUM
eurjchem-336	332	2	(	(	PUNCT
eurjchem-336	332	3	6c	6c	NOUN
eurjchem-336	332	4	):	):	PUNCT
eurjchem-336	332	5	ft‐ir	ft‐ir	NOUN
eurjchem-336	332	6	(	(	PUNCT
eurjchem-336	332	7	kbr	kbr	PROPN
eurjchem-336	332	8	,	,	PUNCT
eurjchem-336	332	9			PROPN
eurjchem-336	332	10	,	,	PUNCT
eurjchem-336	332	11	cm‐1	cm‐1	PROPN
eurjchem-336	332	12	):	):	PUNCT
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eurjchem-336	332	14	.	.	PUNCT
eurjchem-336	333	1	1h	1h	NUM
eurjchem-336	333	2	nmr	nmr	NOUN
eurjchem-336	333	3	(	(	PUNCT
eurjchem-336	333	4	300	300	NUM
eurjchem-336	333	5	mhz	mhz	NOUN
eurjchem-336	333	6	,	,	PUNCT
eurjchem-336	333	7	dmso‐d6	dmso‐d6	NUM
eurjchem-336	333	8	):	):	PUNCT
eurjchem-336	333	9	7.48‐7.51	7.48‐7.51	NUM
eurjchem-336	333	10	(	(	PUNCT
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eurjchem-336	333	14	,	,	PUNCT
eurjchem-336	333	15	ph‐h	ph‐h	PROPN
eurjchem-336	333	16	)	)	PUNCT
eurjchem-336	333	17	,	,	PUNCT
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eurjchem-336	333	20	t	t	PROPN
eurjchem-336	333	21	,	,	PUNCT
eurjchem-336	333	22	2h	2h	NUM
eurjchem-336	333	23	,	,	PUNCT
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eurjchem-336	333	25	=	=	SYM
eurjchem-336	333	26	7.2	7.2	NUM
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eurjchem-336	333	28	,	,	PUNCT
eurjchem-336	333	29	ph‐h	ph‐h	PROPN
eurjchem-336	333	30	)	)	PUNCT
eurjchem-336	333	31	,	,	PUNCT
eurjchem-336	333	32	7.87	7.87	NUM
eurjchem-336	333	33	(	(	PUNCT
eurjchem-336	333	34	d	d	PROPN
eurjchem-336	333	35	,	,	PUNCT
eurjchem-336	333	36	1h	1h	NUM
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eurjchem-336	333	39	=	=	SYM
eurjchem-336	333	40	1.8	1.8	NUM
eurjchem-336	333	41	hz	hz	NOUN
eurjchem-336	333	42	,	,	PUNCT
eurjchem-336	333	43	c7‐h	c7‐h	PROPN
eurjchem-336	333	44	)	)	PUNCT
eurjchem-336	333	45	,	,	PUNCT
eurjchem-336	333	46	7.92	7.92	NUM
eurjchem-336	333	47	(	(	PUNCT
eurjchem-336	333	48	d	d	PROPN
eurjchem-336	333	49	,	,	PUNCT
eurjchem-336	333	50	2h	2h	NUM
eurjchem-336	333	51	,	,	PUNCT
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eurjchem-336	334	1	=	=	SYM
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eurjchem-336	334	4	,	,	PUNCT
eurjchem-336	334	5	ph‐h	ph‐h	PROPN
eurjchem-336	334	6	)	)	PUNCT
eurjchem-336	334	7	,	,	PUNCT
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eurjchem-336	334	10	d	d	PROPN
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eurjchem-336	334	13	,	,	PUNCT
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eurjchem-336	334	15	=	=	SYM
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eurjchem-336	334	17	hz	hz	ADJ
eurjchem-336	334	18	,	,	PUNCT
eurjchem-336	334	19	c9‐h	c9‐h	NOUN
eurjchem-336	334	20	)	)	PUNCT
eurjchem-336	334	21	,	,	PUNCT
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eurjchem-336	334	25	,	,	PUNCT
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eurjchem-336	334	29	)	)	PUNCT
eurjchem-336	334	30	.	.	PUNCT
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eurjchem-336	335	3	(	(	PUNCT
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eurjchem-336	335	6	,	,	PUNCT
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eurjchem-336	335	8	):	):	PUNCT
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eurjchem-336	335	10	,	,	PUNCT
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eurjchem-336	335	16	,	,	PUNCT
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eurjchem-336	335	18	,	,	PUNCT
eurjchem-336	335	19	128.3	128.3	NUM
eurjchem-336	335	20	,	,	PUNCT
eurjchem-336	335	21	131.4	131.4	NUM
eurjchem-336	335	22	,	,	PUNCT
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eurjchem-336	335	24	,	,	PUNCT
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eurjchem-336	335	26	,	,	PUNCT
eurjchem-336	335	27	138.6	138.6	NUM
eurjchem-336	335	28	,	,	PUNCT
eurjchem-336	335	29	138.9	138.9	NUM
eurjchem-336	335	30	,	,	PUNCT
eurjchem-336	335	31	148.0	148.0	NUM
eurjchem-336	335	32	,	,	PUNCT
eurjchem-336	335	33	148.9	148.9	NUM
eurjchem-336	335	34	,	,	PUNCT
eurjchem-336	335	35	156.0	156.0	NUM
eurjchem-336	335	36	.	.	PUNCT
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eurjchem-336	336	2	(	(	PUNCT
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eurjchem-336	336	4	,	,	PUNCT
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eurjchem-336	336	7	z	z	NOUN
eurjchem-336	336	8	):	):	PUNCT
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eurjchem-336	336	10	(	(	PUNCT
eurjchem-336	336	11	m+	m+	NUM
eurjchem-336	336	12	)	)	PUNCT
eurjchem-336	336	13	.	.	PUNCT
eurjchem-336	337	1	anal	anal	PROPN
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eurjchem-336	337	4	.	.	PUNCT
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eurjchem-336	338	2	c16h8n2o2cli	c16h8n2o2cli	PROPN
eurjchem-336	338	3	.	.	PROPN
eurjchem-336	338	4	c	c	X
eurjchem-336	338	5	,	,	PUNCT
eurjchem-336	338	6	45.49	45.49	NUM
eurjchem-336	338	7	;	;	PUNCT
eurjchem-336	338	8	h	h	NOUN
eurjchem-336	338	9	,	,	PUNCT
eurjchem-336	338	10	1.89	1.89	NUM
eurjchem-336	338	11	;	;	PUNCT
eurjchem-336	338	12	n	n	CCONJ
eurjchem-336	338	13	,	,	PUNCT
eurjchem-336	338	14	6.63	6.63	NUM
eurjchem-336	338	15	.	.	PUNCT
eurjchem-336	338	16	found	find	VERB
eurjchem-336	338	17	:	:	PUNCT
eurjchem-336	339	1	c	c	X
eurjchem-336	339	2	,	,	PUNCT
eurjchem-336	339	3	45.41	45.41	NUM
eurjchem-336	339	4	;	;	PUNCT
eurjchem-336	339	5	h	h	X
eurjchem-336	339	6	,	,	PUNCT
eurjchem-336	339	7	1.81	1.81	NUM
eurjchem-336	339	8	;	;	PUNCT
eurjchem-336	339	9	n	n	CCONJ
eurjchem-336	339	10	,	,	PUNCT
eurjchem-336	339	11	6.59	6.59	NUM
eurjchem-336	339	12	%	%	NOUN
eurjchem-336	339	13	.	.	PUNCT
eurjchem-336	340	1	3	3	X
eurjchem-336	340	2	.	.	NOUN
eurjchem-336	340	3	results	result	NOUN
eurjchem-336	340	4	and	and	CCONJ
eurjchem-336	340	5	discussion	discussion	VERB
eurjchem-336	340	6	the	the	DET
eurjchem-336	340	7	overall	overall	ADJ
eurjchem-336	340	8	synthetic	synthetic	ADJ
eurjchem-336	340	9	route	route	NOUN
eurjchem-336	340	10	utilized	utilize	VERB
eurjchem-336	340	11	for	for	ADP
eurjchem-336	340	12	the	the	DET
eurjchem-336	340	13	preparation	preparation	NOUN
eurjchem-336	340	14	of	of	ADP
eurjchem-336	340	15	the	the	DET
eurjchem-336	340	16	target	target	NOUN
eurjchem-336	340	17	pyrazolocoumarin	pyrazolocoumarin	NOUN
eurjchem-336	340	18	is	be	AUX
eurjchem-336	340	19	depicted	depict	VERB
eurjchem-336	340	20	in	in	ADP
eurjchem-336	340	21	scheme	scheme	NOUN
eurjchem-336	340	22	1	1	NUM
eurjchem-336	340	23	and	and	CCONJ
eurjchem-336	340	24	scheme	scheme	NOUN
eurjchem-336	340	25	2	2	NUM
eurjchem-336	340	26	.	.	PUNCT
eurjchem-336	341	1	our	our	PRON
eurjchem-336	341	2	approach	approach	NOUN
eurjchem-336	341	3	to	to	ADP
eurjchem-336	341	4	the	the	DET
eurjchem-336	341	5	synthesis	synthesis	NOUN
eurjchem-336	341	6	of	of	ADP
eurjchem-336	341	7	the	the	DET
eurjchem-336	341	8	target	target	NOUN
eurjchem-336	341	9	molecule	molecule	NOUN
eurjchem-336	341	10	,	,	PUNCT
eurjchem-336	341	11	started	start	VERB
eurjchem-336	341	12	from	from	ADP
eurjchem-336	341	13	the	the	DET
eurjchem-336	341	14	condensation	condensation	NOUN
eurjchem-336	341	15	of	of	ADP
eurjchem-336	341	16	halo	halo	NOUN
eurjchem-336	341	17	substituted	substitute	VERB
eurjchem-336	341	18	o‐	o‐	PROPN
eurjchem-336	341	19	hydroxyacetophenones	hydroxyacetophenone	NOUN
eurjchem-336	341	20	,	,	PUNCT
eurjchem-336	341	21	1a‐g	1a‐g	NOUN
eurjchem-336	341	22	,	,	PUNCT
eurjchem-336	341	23	with	with	SCONJ
eurjchem-336	341	24	phenyl	phenyl	NOUN
eurjchem-336	341	25	hydrazine	hydrazine	NOUN
eurjchem-336	341	26	to	to	PART
eurjchem-336	341	27	efficiently	efficiently	ADV
eurjchem-336	341	28	provide	provide	VERB
eurjchem-336	341	29	the	the	DET
eurjchem-336	341	30	hydrazones	hydrazone	NOUN
eurjchem-336	341	31	,	,	PUNCT
eurjchem-336	341	32	2a‐g	2a‐g	NOUN
eurjchem-336	341	33	.	.	PUNCT
eurjchem-336	342	1	these	these	DET
eurjchem-336	342	2	derivatives	derivative	NOUN
eurjchem-336	342	3	were	be	AUX
eurjchem-336	342	4	purified	purify	VERB
eurjchem-336	342	5	and	and	CCONJ
eurjchem-336	342	6	transformed	transform	VERB
eurjchem-336	342	7	into	into	ADP
eurjchem-336	342	8	the	the	DET
eurjchem-336	342	9	corresponding	correspond	VERB
eurjchem-336	342	10	3‐(2‐	3‐(2‐	NUM
eurjchem-336	342	11	hydroxyaryl)‐1‐phenyl‐1h‐pyrazole‐4‐carbaldehydes	hydroxyaryl)‐1‐phenyl‐1h‐pyrazole‐4‐carbaldehyde	NOUN
eurjchem-336	342	12	,	,	PUNCT
eurjchem-336	342	13	3a‐g	3a‐g	NOUN
eurjchem-336	342	14	,	,	PUNCT
eurjchem-336	342	15	by	by	ADP
eurjchem-336	342	16	using	use	VERB
eurjchem-336	342	17	the	the	DET
eurjchem-336	342	18	vilsmeier	vilsmeier	ADJ
eurjchem-336	342	19	reagent	reagent	NOUN
eurjchem-336	342	20	(	(	PUNCT
eurjchem-336	342	21	according	accord	VERB
eurjchem-336	342	22	to	to	ADP
eurjchem-336	342	23	method	method	NOUN
eurjchem-336	342	24	of	of	ADP
eurjchem-336	342	25	rathelot	rathelot	NOUN
eurjchem-336	342	26	et	et	NOUN
eurjchem-336	342	27	.	.	PUNCT
eurjchem-336	343	1	al	al	PROPN
eurjchem-336	343	2	.	.	PUNCT
eurjchem-336	344	1	[	[	X
eurjchem-336	344	2	34	34	NUM
eurjchem-336	344	3	]	]	PUNCT
eurjchem-336	344	4	)	)	PUNCT
eurjchem-336	344	5	.	.	PUNCT
eurjchem-336	345	1	the	the	DET
eurjchem-336	345	2	3‐(2‐(allyloxyaryl)‐1‐phenyl‐1h‐pyrazole‐4‐	3‐(2‐(allyloxyaryl)‐1‐phenyl‐1h‐pyrazole‐4‐	NUM
eurjchem-336	345	3	carbaldehydes	carbaldehyde	NOUN
eurjchem-336	345	4	,	,	PUNCT
eurjchem-336	345	5	4a‐g	4a‐g	NOUN
eurjchem-336	345	6	,	,	PUNCT
eurjchem-336	345	7	were	be	AUX
eurjchem-336	345	8	readily	readily	ADV
eurjchem-336	345	9	prepared	prepare	VERB
eurjchem-336	345	10	from	from	ADP
eurjchem-336	345	11	3a‐g	3a‐g	NOUN
eurjchem-336	345	12	using	use	VERB
eurjchem-336	345	13	the	the	DET
eurjchem-336	345	14	ally	ally	NOUN
eurjchem-336	345	15	bromide	bromide	NOUN
eurjchem-336	345	16	in	in	ADP
eurjchem-336	345	17	dmso	dmso	NOUN
eurjchem-336	345	18	(	(	PUNCT
eurjchem-336	345	19	scheme	scheme	NOUN
eurjchem-336	345	20	1	1	NUM
eurjchem-336	345	21	)	)	PUNCT
eurjchem-336	345	22	.	.	PUNCT
eurjchem-336	346	1	these	these	DET
eurjchem-336	346	2	key	key	ADJ
eurjchem-336	346	3	intermediate	intermediate	ADJ
eurjchem-336	346	4	substituted	substitute	VERB
eurjchem-336	346	5	pyrazole‐4‐carbaldehydes	pyrazole‐4‐carbaldehyde	NOUN
eurjchem-336	346	6	(	(	PUNCT
eurjchem-336	346	7	3a‐g	3a‐g	NOUN
eurjchem-336	346	8	&	&	CCONJ
eurjchem-336	346	9	4a‐g	4a‐g	PROPN
eurjchem-336	346	10	)	)	PUNCT
eurjchem-336	346	11	were	be	AUX
eurjchem-336	346	12	required	require	VERB
eurjchem-336	346	13	for	for	ADP
eurjchem-336	346	14	the	the	DET
eurjchem-336	346	15	synthesis	synthesis	NOUN
eurjchem-336	346	16	of	of	ADP
eurjchem-336	346	17	2‐arylpyrazolo[4,3‐c]coumarins	2‐arylpyrazolo[4,3‐c]coumarins	NUM
eurjchem-336	346	18	.	.	PUNCT
eurjchem-336	347	1	scheme	scheme	NOUN
eurjchem-336	347	2	1	1	NUM
eurjchem-336	347	3	scheme	scheme	NOUN
eurjchem-336	347	4	2	2	NUM
eurjchem-336	347	5	lokhande	lokhande	NOUN
eurjchem-336	347	6	et	et	PROPN
eurjchem-336	347	7	al	al	PROPN
eurjchem-336	347	8	.	.	PUNCT
eurjchem-336	347	9	/	/	SYM
eurjchem-336	347	10	european	european	PROPN
eurjchem-336	347	11	journal	journal	PROPN
eurjchem-336	347	12	of	of	ADP
eurjchem-336	347	13	chemistry	chemistry	NOUN
eurjchem-336	347	14	2	2	NUM
eurjchem-336	347	15	(	(	PUNCT
eurjchem-336	347	16	2	2	NUM
eurjchem-336	347	17	)	)	PUNCT
eurjchem-336	347	18	(	(	PUNCT
eurjchem-336	347	19	2011	2011	NUM
eurjchem-336	347	20	)	)	PUNCT
eurjchem-336	347	21	223‐228	223‐228	NUM
eurjchem-336	347	22	227	227	NUM
eurjchem-336	347	23	r1	r1	PROPN
eurjchem-336	347	24	r2	r2	PROPN
eurjchem-336	347	25	r1	r1	PROPN
eurjchem-336	347	26	r2	r2	PROPN
eurjchem-336	347	27	r1	r1	PROPN
eurjchem-336	347	28	r2	r2	PROPN
eurjchem-336	347	29	r1	r1	PROPN
eurjchem-336	347	30	r2	r2	PROPN
eurjchem-336	347	31	3a	3a	PROPN
eurjchem-336	347	32	h	h	PROPN
eurjchem-336	347	33	cl	cl	NOUN
eurjchem-336	347	34	4a	4a	NUM
eurjchem-336	347	35	h	h	NOUN
eurjchem-336	347	36	cl	cl	NOUN
eurjchem-336	347	37	5a	5a	NUM
eurjchem-336	347	38	h	h	NOUN
eurjchem-336	347	39	cl	cl	NOUN
eurjchem-336	347	40	6a	6a	NOUN
eurjchem-336	348	1	i	i	PRON
eurjchem-336	348	2	cl	cl	VERB
eurjchem-336	349	1	3b	3b	NUM
eurjchem-336	349	2	h	h	NOUN
eurjchem-336	349	3	br	br	PROPN
eurjchem-336	349	4	4b	4b	PROPN
eurjchem-336	349	5	h	h	NOUN
eurjchem-336	349	6	br	br	PROPN
eurjchem-336	349	7	5b	5b	NUM
eurjchem-336	349	8	h	h	NOUN
eurjchem-336	349	9	br	br	NOUN
eurjchem-336	350	1	6b	6b	NOUN
eurjchem-336	351	1	i	i	PRON
eurjchem-336	351	2	br	br	VERB
eurjchem-336	351	3	3c	3c	NUM
eurjchem-336	351	4	cl	cl	NOUN
eurjchem-336	351	5	h	h	NOUN
eurjchem-336	351	6	4c	4c	NUM
eurjchem-336	352	1	cl	cl	NOUN
eurjchem-336	352	2	h	h	NOUN
eurjchem-336	352	3	5c	5c	NUM
eurjchem-336	352	4	cl	cl	NOUN
eurjchem-336	352	5	h	h	NOUN
eurjchem-336	352	6	6c	6c	NOUN
eurjchem-336	352	7	cl	cl	NOUN
eurjchem-336	353	1	i	i	PRON
eurjchem-336	353	2	3d	3d	NUM
eurjchem-336	353	3	cl	cl	NOUN
eurjchem-336	353	4	cl	cl	NOUN
eurjchem-336	353	5	4d	4d	NUM
eurjchem-336	353	6	cl	cl	NOUN
eurjchem-336	353	7	cl	cl	NOUN
eurjchem-336	353	8	5d	5d	ADJ
eurjchem-336	353	9	cl	cl	NOUN
eurjchem-336	353	10	cl	cl	NOUN
eurjchem-336	354	1	3e	3e	X
eurjchem-336	354	2	br	br	NOUN
eurjchem-336	355	1	br	br	PROPN
eurjchem-336	355	2	4e	4e	PROPN
eurjchem-336	355	3	br	br	PROPN
eurjchem-336	355	4	br	br	PROPN
eurjchem-336	355	5	5e	5e	PROPN
eurjchem-336	356	1	br	br	INTJ
eurjchem-336	356	2	br	br	PROPN
eurjchem-336	356	3	3f	3f	PROPN
eurjchem-336	356	4	br	br	PROPN
eurjchem-336	356	5	cl	cl	NOUN
eurjchem-336	356	6	4f	4f	NUM
eurjchem-336	356	7	br	br	NOUN
eurjchem-336	356	8	cl	cl	NOUN
eurjchem-336	356	9	5f	5f	NOUN
eurjchem-336	356	10	br	br	NOUN
eurjchem-336	356	11	cl	cl	NOUN
eurjchem-336	357	1	3	3	NUM
eurjchem-336	357	2	g	g	NOUN
eurjchem-336	357	3	br	br	NOUN
eurjchem-336	357	4	me	i	PRON
eurjchem-336	357	5	4	4	NUM
eurjchem-336	357	6	g	g	NOUN
eurjchem-336	357	7	br	br	NOUN
eurjchem-336	357	8	me	i	PRON
eurjchem-336	357	9	5	5	NUM
eurjchem-336	357	10	g	g	NOUN
eurjchem-336	357	11	br	br	VERB
eurjchem-336	357	12	me	i	PRON
eurjchem-336	357	13	(	(	PUNCT
eurjchem-336	357	14	a	a	NOUN
eurjchem-336	357	15	)	)	PUNCT
eurjchem-336	357	16	i2	i2	NOUN
eurjchem-336	357	17	(	(	PUNCT
eurjchem-336	357	18	10	10	NUM
eurjchem-336	357	19	mol	mol	ADP
eurjchem-336	357	20	%	%	NOUN
eurjchem-336	357	21	)	)	PUNCT
eurjchem-336	357	22	/dmso	/dmso	ADJ
eurjchem-336	357	23	,	,	PUNCT
eurjchem-336	357	24	conc	conc	NOUN
eurjchem-336	357	25	.	.	PUNCT
eurjchem-336	358	1	h2so4	h2so4	PROPN
eurjchem-336	358	2	,	,	PUNCT
eurjchem-336	358	3	120	120	NUM
eurjchem-336	358	4	oc	oc	NOUN
eurjchem-336	358	5	,	,	PUNCT
eurjchem-336	358	6	5‐7	5‐7	PROPN
eurjchem-336	358	7	h.	h.	NOUN
eurjchem-336	358	8	(	(	PUNCT
eurjchem-336	358	9	b	b	X
eurjchem-336	358	10	)	)	PUNCT
eurjchem-336	358	11	i2	i2	NOUN
eurjchem-336	358	12	(	(	PUNCT
eurjchem-336	358	13	1.2	1.2	NUM
eurjchem-336	358	14	equiv.)/dmso	equiv.)/dmso	ADJ
eurjchem-336	358	15	,	,	PUNCT
eurjchem-336	358	16	conc	conc	NOUN
eurjchem-336	358	17	.	.	PUNCT
eurjchem-336	359	1	h2so4	h2so4	PROPN
eurjchem-336	359	2	,	,	PUNCT
eurjchem-336	359	3	120	120	NUM
eurjchem-336	359	4	oc	oc	NOUN
eurjchem-336	359	5	,	,	PUNCT
eurjchem-336	359	6	3‐4	3‐4	PROPN
eurjchem-336	359	7	h.	h.	PROPN
eurjchem-336	359	8	scheme	scheme	PROPN
eurjchem-336	359	9	3	3	NUM
eurjchem-336	359	10	initially	initially	ADV
eurjchem-336	359	11	,	,	PUNCT
eurjchem-336	359	12	we	we	PRON
eurjchem-336	359	13	attempted	attempt	VERB
eurjchem-336	359	14	the	the	DET
eurjchem-336	359	15	oxidative	oxidative	ADJ
eurjchem-336	359	16	cyclization	cyclization	NOUN
eurjchem-336	359	17	of	of	ADP
eurjchem-336	359	18	3‐(3,5‐	3‐(3,5‐	NUM
eurjchem-336	359	19	dichloro‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐pyrazole‐4‐carbalde‐	dichloro‐2‐hydroxyphenyl)‐1‐phenyl‐1h‐pyrazole‐4‐carbalde‐	PROPN
eurjchem-336	359	20	hyde	hyde	PROPN
eurjchem-336	359	21	,	,	PUNCT
eurjchem-336	359	22	3d	3d	NUM
eurjchem-336	359	23	,	,	PUNCT
eurjchem-336	359	24	using	use	VERB
eurjchem-336	359	25	iodine	iodine	NOUN
eurjchem-336	359	26	(	(	PUNCT
eurjchem-336	359	27	5	5	NUM
eurjchem-336	359	28	%	%	NOUN
eurjchem-336	359	29	)	)	PUNCT
eurjchem-336	359	30	in	in	ADP
eurjchem-336	359	31	dimethylsulfoxide	dimethylsulfoxide	ADV
eurjchem-336	359	32	in	in	ADP
eurjchem-336	359	33	the	the	DET
eurjchem-336	359	34	presence	presence	NOUN
eurjchem-336	359	35	of	of	ADP
eurjchem-336	359	36	h2so4	h2so4	PROPN
eurjchem-336	359	37	at	at	ADP
eurjchem-336	359	38	60	60	NUM
eurjchem-336	359	39	oc	oc	NOUN
eurjchem-336	359	40	as	as	ADP
eurjchem-336	359	41	per	per	ADP
eurjchem-336	359	42	our	our	PRON
eurjchem-336	359	43	known	know	VERB
eurjchem-336	359	44	procedures	procedure	NOUN
eurjchem-336	359	45	for	for	ADP
eurjchem-336	359	46	the	the	DET
eurjchem-336	359	47	flavone	flavone	ADJ
eurjchem-336	359	48	synthesis	synthesis	NOUN
eurjchem-336	359	49	[	[	X
eurjchem-336	359	50	23	23	NUM
eurjchem-336	359	51	]	]	PUNCT
eurjchem-336	359	52	.	.	PUNCT
eurjchem-336	360	1	the	the	DET
eurjchem-336	360	2	product	product	NOUN
eurjchem-336	360	3	was	be	AUX
eurjchem-336	360	4	not	not	PART
eurjchem-336	360	5	appearing	appear	VERB
eurjchem-336	360	6	even	even	ADV
eurjchem-336	360	7	after	after	ADP
eurjchem-336	360	8	30	30	NUM
eurjchem-336	360	9	h.	h.	NOUN
eurjchem-336	360	10	showing	show	VERB
eurjchem-336	360	11	that	that	SCONJ
eurjchem-336	360	12	the	the	DET
eurjchem-336	360	13	formyl	formyl	ADJ
eurjchem-336	360	14	group	group	NOUN
eurjchem-336	360	15	of	of	ADP
eurjchem-336	360	16	the	the	DET
eurjchem-336	360	17	pyrazole	pyrazole	NOUN
eurjchem-336	360	18	is	be	AUX
eurjchem-336	360	19	not	not	PART
eurjchem-336	360	20	reactive	reactive	ADJ
eurjchem-336	360	21	.	.	PUNCT
eurjchem-336	361	1	actually	actually	ADV
eurjchem-336	361	2	the	the	DET
eurjchem-336	361	3	reaction	reaction	NOUN
eurjchem-336	361	4	rate	rate	NOUN
eurjchem-336	361	5	depended	depend	VERB
eurjchem-336	361	6	on	on	ADP
eurjchem-336	361	7	the	the	DET
eurjchem-336	361	8	catalyst	catalyst	NOUN
eurjchem-336	361	9	amount	amount	NOUN
eurjchem-336	361	10	and	and	CCONJ
eurjchem-336	361	11	temperature	temperature	NOUN
eurjchem-336	361	12	(	(	PUNCT
eurjchem-336	361	13	scheme	scheme	NOUN
eurjchem-336	361	14	2	2	NUM
eurjchem-336	361	15	,	,	PUNCT
eurjchem-336	361	16	table	table	NOUN
eurjchem-336	361	17	1	1	NUM
eurjchem-336	361	18	)	)	PUNCT
eurjchem-336	361	19	.	.	PUNCT
eurjchem-336	362	1	the	the	DET
eurjchem-336	362	2	best	good	ADJ
eurjchem-336	362	3	condition	condition	NOUN
eurjchem-336	362	4	was	be	AUX
eurjchem-336	362	5	obtained	obtain	VERB
eurjchem-336	362	6	,	,	PUNCT
eurjchem-336	362	7	using	use	VERB
eurjchem-336	362	8	of	of	ADP
eurjchem-336	362	9	10	10	NUM
eurjchem-336	362	10	%	%	NOUN
eurjchem-336	362	11	iodine	iodine	NOUN
eurjchem-336	362	12	in	in	ADP
eurjchem-336	362	13	dmso	dmso	NOUN
eurjchem-336	362	14	in	in	ADP
eurjchem-336	362	15	the	the	DET
eurjchem-336	362	16	presence	presence	NOUN
eurjchem-336	362	17	of	of	ADP
eurjchem-336	362	18	catalytic	catalytic	ADJ
eurjchem-336	362	19	amount	amount	NOUN
eurjchem-336	362	20	of	of	ADP
eurjchem-336	362	21	h2so4	h2so4	NOUN
eurjchem-336	362	22	at	at	ADP
eurjchem-336	362	23	120	120	NUM
eurjchem-336	362	24	oc	oc	NOUN
eurjchem-336	362	25	,	,	PUNCT
eurjchem-336	362	26	and	and	CCONJ
eurjchem-336	362	27	the	the	DET
eurjchem-336	362	28	reaction	reaction	NOUN
eurjchem-336	362	29	went	go	VERB
eurjchem-336	362	30	to	to	ADP
eurjchem-336	362	31	completion	completion	NOUN
eurjchem-336	362	32	within	within	ADP
eurjchem-336	362	33	5	5	NUM
eurjchem-336	362	34	h	h	NOUN
eurjchem-336	362	35	and	and	CCONJ
eurjchem-336	362	36	the	the	DET
eurjchem-336	362	37	corresponding	corresponding	ADJ
eurjchem-336	362	38	product	product	NOUN
eurjchem-336	362	39	5d	5d	NUM
eurjchem-336	362	40	was	be	AUX
eurjchem-336	362	41	obtained	obtain	VERB
eurjchem-336	362	42	in	in	ADP
eurjchem-336	362	43	92	92	NUM
eurjchem-336	362	44	%	%	NOUN
eurjchem-336	362	45	yield	yield	NOUN
eurjchem-336	362	46	(	(	PUNCT
eurjchem-336	362	47	table	table	NOUN
eurjchem-336	362	48	1	1	NUM
eurjchem-336	362	49	)	)	PUNCT
eurjchem-336	362	50	.	.	PUNCT
eurjchem-336	363	1	encouraged	encourage	VERB
eurjchem-336	363	2	based	base	VERB
eurjchem-336	363	3	on	on	ADP
eurjchem-336	363	4	these	these	DET
eurjchem-336	363	5	results	result	NOUN
eurjchem-336	363	6	,	,	PUNCT
eurjchem-336	363	7	various	various	ADJ
eurjchem-336	363	8	4‐formylpyrazoles	4‐formylpyrazole	NOUN
eurjchem-336	363	9	were	be	AUX
eurjchem-336	363	10	converted	convert	VERB
eurjchem-336	363	11	to	to	ADP
eurjchem-336	363	12	the	the	DET
eurjchem-336	363	13	corresponding	corresponding	ADJ
eurjchem-336	363	14	coumarins	coumarin	NOUN
eurjchem-336	363	15	in	in	ADP
eurjchem-336	363	16	87‐94	87‐94	NUM
eurjchem-336	363	17	%	%	NOUN
eurjchem-336	363	18	yield	yield	NOUN
eurjchem-336	363	19	(	(	PUNCT
eurjchem-336	363	20	scheme	scheme	NOUN
eurjchem-336	363	21	3	3	NUM
eurjchem-336	363	22	,	,	PUNCT
eurjchem-336	363	23	table	table	NOUN
eurjchem-336	363	24	2	2	NUM
eurjchem-336	363	25	)	)	PUNCT
eurjchem-336	363	26	.	.	PUNCT
eurjchem-336	364	1	the	the	DET
eurjchem-336	364	2	reaction	reaction	NOUN
eurjchem-336	364	3	probably	probably	ADV
eurjchem-336	364	4	proceeds	proceed	VERB
eurjchem-336	364	5	via	via	ADP
eurjchem-336	364	6	formation	formation	NOUN
eurjchem-336	364	7	of	of	ADP
eurjchem-336	364	8	hemiacetals	hemiacetal	NOUN
eurjchem-336	364	9	by	by	ADP
eurjchem-336	364	10	the	the	DET
eurjchem-336	364	11	reaction	reaction	NOUN
eurjchem-336	364	12	of	of	ADP
eurjchem-336	364	13	4‐formyl	4‐formyl	NUM
eurjchem-336	364	14	group	group	NOUN
eurjchem-336	364	15	and	and	CCONJ
eurjchem-336	364	16	phenol	phenol	NOUN
eurjchem-336	364	17	,	,	PUNCT
eurjchem-336	364	18	and	and	CCONJ
eurjchem-336	364	19	the	the	DET
eurjchem-336	364	20	oxidation	oxidation	NOUN
eurjchem-336	364	21	of	of	ADP
eurjchem-336	364	22	hemiacetal	hemiacetal	NOUN
eurjchem-336	364	23	to	to	ADP
eurjchem-336	364	24	lactone	lactone	NOUN
eurjchem-336	364	25	by	by	ADP
eurjchem-336	364	26	molecular	molecular	ADJ
eurjchem-336	364	27	iodine	iodine	NOUN
eurjchem-336	364	28	in	in	ADP
eurjchem-336	364	29	dimethylsulfoxide	dimethylsulfoxide	ADJ
eurjchem-336	364	30	.	.	PUNCT
eurjchem-336	364	31	table	table	NOUN
eurjchem-336	365	1	1	1	NUM
eurjchem-336	365	2	.	.	PUNCT
eurjchem-336	365	3	effect	effect	NOUN
eurjchem-336	365	4	of	of	ADP
eurjchem-336	365	5	the	the	DET
eurjchem-336	365	6	catalyst	catalyst	NOUN
eurjchem-336	365	7	iodine	iodine	NOUN
eurjchem-336	365	8	and	and	CCONJ
eurjchem-336	365	9	temperature	temperature	NOUN
eurjchem-336	365	10	on	on	ADP
eurjchem-336	365	11	the	the	DET
eurjchem-336	365	12	synthesis	synthesis	NOUN
eurjchem-336	365	13	of	of	ADP
eurjchem-336	365	14	6,8‐	6,8‐	NUM
eurjchem-336	365	15	dichloro‐2‐phenylchromeno[4,3‐c]pyrazol‐4(2h)‐one	dichloro‐2‐phenylchromeno[4,3‐c]pyrazol‐4(2h)‐one	PROPN
eurjchem-336	365	16	(	(	PUNCT
eurjchem-336	365	17	4d	4d	NUM
eurjchem-336	365	18	)	)	PUNCT
eurjchem-336	365	19	.	.	PUNCT
eurjchem-336	366	1	yield	yield	NOUN
eurjchem-336	366	2	(	(	PUNCT
eurjchem-336	366	3	%	%	NOUN
eurjchem-336	366	4	)	)	PUNCT
eurjchem-336	366	5	time	time	NOUN
eurjchem-336	366	6	(	(	PUNCT
eurjchem-336	366	7	h	h	NOUN
eurjchem-336	366	8	)	)	PUNCT
eurjchem-336	366	9	temp	temp	NOUN
eurjchem-336	366	10	(	(	PUNCT
eurjchem-336	366	11	oc)mol	oc)mol	PROPN
eurjchem-336	366	12	(	(	PUNCT
eurjchem-336	366	13	%	%	NOUN
eurjchem-336	366	14	)	)	PUNCT
eurjchem-336	366	15	entry	entry	NOUN
eurjchem-336	366	16	nr30	nr30	PROPN
eurjchem-336	366	17	rt	rt	PROPN
eurjchem-336	366	18	5	5	NUM
eurjchem-336	366	19	1	1	NUM
eurjchem-336	366	20	nr30	nr30	PROPN
eurjchem-336	366	21	rt	rt	PROPN
eurjchem-336	366	22	10	10	NUM
eurjchem-336	366	23	2	2	NUM
eurjchem-336	366	24	nr30	nr30	PROPN
eurjchem-336	366	25	rt	rt	PROPN
eurjchem-336	366	26	15	15	NUM
eurjchem-336	366	27	3	3	NUM
eurjchem-336	366	28	nr30	nr30	PROPN
eurjchem-336	366	29	rt	rt	PROPN
eurjchem-336	366	30	20	20	NUM
eurjchem-336	366	31	4	4	NUM
eurjchem-336	367	1	nr30	nr30	PROPN
eurjchem-336	367	2	60	60	NUM
eurjchem-336	367	3	5	5	NUM
eurjchem-336	367	4	5	5	NUM
eurjchem-336	367	5	nr30	nr30	PROPN
eurjchem-336	367	6	60	60	NUM
eurjchem-336	367	7	10	10	NUM
eurjchem-336	367	8	6	6	NUM
eurjchem-336	367	9	nr30	nr30	PROPN
eurjchem-336	367	10	60	60	NUM
eurjchem-336	367	11	15	15	NUM
eurjchem-336	367	12	7	7	NUM
eurjchem-336	367	13	2026	2026	NUM
eurjchem-336	367	14	60	60	NUM
eurjchem-336	367	15	20	20	NUM
eurjchem-336	367	16	8	8	NUM
eurjchem-336	367	17	6020	6020	NUM
eurjchem-336	367	18	120	120	NUM
eurjchem-336	367	19	5	5	NUM
eurjchem-336	367	20	9	9	NUM
eurjchem-336	367	21	925	925	NUM
eurjchem-336	367	22	120	120	NUM
eurjchem-336	367	23	10	10	NUM
eurjchem-336	367	24	10	10	NUM
eurjchem-336	367	25	rt	rt	NOUN
eurjchem-336	367	26	:	:	PUNCT
eurjchem-336	367	27	room	room	NOUN
eurjchem-336	367	28	temperature	temperature	NOUN
eurjchem-336	367	29	.	.	PUNCT
eurjchem-336	368	1	nr	nr	PRON
eurjchem-336	368	2	:	:	PUNCT
eurjchem-336	368	3	no	no	DET
eurjchem-336	368	4	reaction	reaction	NOUN
eurjchem-336	368	5	.	.	PUNCT
eurjchem-336	369	1	according	accord	VERB
eurjchem-336	369	2	to	to	ADP
eurjchem-336	369	3	our	our	PRON
eurjchem-336	369	4	research	research	NOUN
eurjchem-336	369	5	in	in	ADP
eurjchem-336	369	6	deallylation	deallylation	NOUN
eurjchem-336	369	7	of	of	ADP
eurjchem-336	369	8	2'‐	2'‐	NUM
eurjchem-336	369	9	allyloxychalcones	allyloxychalcone	NOUN
eurjchem-336	369	10	[	[	X
eurjchem-336	369	11	30	30	NUM
eurjchem-336	369	12	]	]	PUNCT
eurjchem-336	369	13	,	,	PUNCT
eurjchem-336	369	14	we	we	PRON
eurjchem-336	369	15	attempted	attempt	VERB
eurjchem-336	369	16	to	to	PART
eurjchem-336	369	17	apply	apply	VERB
eurjchem-336	369	18	this	this	DET
eurjchem-336	369	19	reagent	reagent	NOUN
eurjchem-336	369	20	for	for	ADP
eurjchem-336	369	21	3‐(2‐(allyloxyaryl)‐1‐phenyl‐1h‐pyrazole‐4‐carbaldehydes	3‐(2‐(allyloxyaryl)‐1‐phenyl‐1h‐pyrazole‐4‐carbaldehydes	NUM
eurjchem-336	369	22	,	,	PUNCT
eurjchem-336	369	23	4a‐	4a‐	NUM
eurjchem-336	369	24	g.	g.	NOUN
eurjchem-336	369	25	in	in	ADP
eurjchem-336	369	26	this	this	DET
eurjchem-336	369	27	case	case	NOUN
eurjchem-336	369	28	also	also	ADV
eurjchem-336	369	29	4a‐g	4a‐g	PROPN
eurjchem-336	369	30	interestingly	interestingly	ADV
eurjchem-336	369	31	easily	easily	ADV
eurjchem-336	369	32	under	under	ADP
eurjchem-336	369	33	went	go	VERB
eurjchem-336	369	34	to	to	PART
eurjchem-336	369	35	deallylation	deallylation	VERB
eurjchem-336	369	36	as	as	ADV
eurjchem-336	369	37	well	well	ADV
eurjchem-336	369	38	as	as	ADP
eurjchem-336	369	39	cyclization	cyclization	NOUN
eurjchem-336	369	40	,	,	PUNCT
eurjchem-336	369	41	and	and	CCONJ
eurjchem-336	369	42	gave	give	VERB
eurjchem-336	369	43	the	the	DET
eurjchem-336	369	44	corresponding	corresponding	ADJ
eurjchem-336	369	45	pyrazolocoumarin	pyrazolocoumarin	NOUN
eurjchem-336	369	46	(	(	PUNCT
eurjchem-336	369	47	scheme	scheme	NOUN
eurjchem-336	369	48	3	3	NUM
eurjchem-336	369	49	)	)	PUNCT
eurjchem-336	369	50	.	.	PUNCT
eurjchem-336	370	1	table	table	NOUN
eurjchem-336	370	2	2	2	NUM
eurjchem-336	370	3	.	.	PUNCT
eurjchem-336	370	4	physico‐chemical	physico‐chemical	ADJ
eurjchem-336	370	5	data	datum	NOUN
eurjchem-336	370	6	of	of	ADP
eurjchem-336	370	7	2‐arylpyrazolo[4,3‐c]coumarins	2‐arylpyrazolo[4,3‐c]coumarins	NUM
eurjchem-336	370	8	.	.	PUNCT
eurjchem-336	371	1	entry	entry	NOUN
eurjchem-336	371	2	r1	r1	PROPN
eurjchem-336	371	3	r2	r2	PROPN
eurjchem-336	371	4	m.p	m.p	PROPN
eurjchem-336	371	5	.	.	PUNCT
eurjchem-336	372	1	(	(	PUNCT
eurjchem-336	372	2	oc	oc	PROPN
eurjchem-336	372	3	)	)	PUNCT
eurjchem-336	372	4	yield	yield	NOUN
eurjchem-336	372	5	(	(	PUNCT
eurjchem-336	372	6	%	%	NOUN
eurjchem-336	372	7	)	)	PUNCT
eurjchem-336	372	8	time	time	NOUN
eurjchem-336	372	9	(	(	PUNCT
eurjchem-336	372	10	h	h	NOUN
eurjchem-336	372	11	)	)	PUNCT
eurjchem-336	372	12	5a	5a	NUM
eurjchem-336	372	13	h	h	NOUN
eurjchem-336	372	14	cl	cl	NOUN
eurjchem-336	372	15	189‐190	189‐190	NUM
eurjchem-336	372	16	89	89	NUM
eurjchem-336	372	17	a	a	PRON
eurjchem-336	372	18	,	,	PUNCT
eurjchem-336	372	19	91b	91b	NUM
eurjchem-336	372	20	7	7	NUM
eurjchem-336	372	21	5b	5b	NUM
eurjchem-336	372	22	h	h	NOUN
eurjchem-336	372	23	br	br	NOUN
eurjchem-336	372	24	196‐197	196‐197	NUM
eurjchem-336	372	25	91	91	NUM
eurjchem-336	372	26	a	a	PRON
eurjchem-336	372	27	,	,	PUNCT
eurjchem-336	372	28	89b	89b	NOUN
eurjchem-336	372	29	6.5	6.5	NUM
eurjchem-336	372	30	5c	5c	NUM
eurjchem-336	372	31	cl	cl	NOUN
eurjchem-336	372	32	h	h	NOUN
eurjchem-336	372	33	183‐184	183‐184	NOUN
eurjchem-336	372	34	93	93	NUM
eurjchem-336	372	35	a	a	PRON
eurjchem-336	372	36	,	,	PUNCT
eurjchem-336	372	37	88b	88b	NOUN
eurjchem-336	372	38	7	7	NUM
eurjchem-336	372	39	5d	5d	NUM
eurjchem-336	372	40	cl	cl	NOUN
eurjchem-336	372	41	cl	cl	NOUN
eurjchem-336	372	42	233‐234	233‐234	NUM
eurjchem-336	372	43	92	92	NUM
eurjchem-336	372	44	a	a	PRON
eurjchem-336	372	45	,	,	PUNCT
eurjchem-336	372	46	88b	88b	NOUN
eurjchem-336	372	47	5	5	NUM
eurjchem-336	372	48	5e	5e	NOUN
eurjchem-336	372	49	br	br	INTJ
eurjchem-336	373	1	br	br	NOUN
eurjchem-336	373	2	248‐249	248‐249	PROPN
eurjchem-336	373	3	88	88	NUM
eurjchem-336	374	1	a	a	DET
eurjchem-336	374	2	,	,	PUNCT
eurjchem-336	374	3	89b	89b	NOUN
eurjchem-336	374	4	5	5	NUM
eurjchem-336	374	5	5f	5f	NOUN
eurjchem-336	374	6	br	br	NOUN
eurjchem-336	374	7	cl	cl	NOUN
eurjchem-336	374	8	258‐259	258‐259	NUM
eurjchem-336	374	9	92	92	NUM
eurjchem-336	374	10	a	a	PRON
eurjchem-336	374	11	,	,	PUNCT
eurjchem-336	374	12	87b	87b	NUM
eurjchem-336	374	13	5.5	5.5	NUM
eurjchem-336	374	14	5	5	NUM
eurjchem-336	374	15	g	g	NOUN
eurjchem-336	374	16	br	br	NOUN
eurjchem-336	374	17	me	i	PRON
eurjchem-336	374	18	254‐255	254‐255	NUM
eurjchem-336	374	19	94	94	NUM
eurjchem-336	375	1	a	a	DET
eurjchem-336	375	2	,	,	PUNCT
eurjchem-336	375	3	88b	88b	NOUN
eurjchem-336	375	4	5	5	NUM
eurjchem-336	375	5	6a	6a	NOUN
eurjchem-336	375	6	i	i	PRON
eurjchem-336	375	7	cl	cl	VERB
eurjchem-336	375	8	203‐204	203‐204	NUM
eurjchem-336	375	9	87	87	NUM
eurjchem-336	375	10	a	a	PRON
eurjchem-336	375	11	,	,	PUNCT
eurjchem-336	375	12	87b	87b	NUM
eurjchem-336	375	13	3.5	3.5	NUM
eurjchem-336	375	14	6b	6b	NUM
eurjchem-336	376	1	i	i	PRON
eurjchem-336	376	2	br	br	VERB
eurjchem-336	376	3	259‐260	259‐260	NUM
eurjchem-336	376	4	89	89	NUM
eurjchem-336	376	5	a	a	PRON
eurjchem-336	376	6	,	,	PUNCT
eurjchem-336	376	7	87b	87b	NUM
eurjchem-336	376	8	3	3	NUM
eurjchem-336	376	9	6c	6c	NUM
eurjchem-336	376	10	cl	cl	NOUN
eurjchem-336	377	1	i	i	PRON
eurjchem-336	377	2	208‐209	208‐209	VERB
eurjchem-336	377	3	91	91	NUM
eurjchem-336	377	4	a	a	PRON
eurjchem-336	377	5	,	,	PUNCT
eurjchem-336	377	6	86b	86b	NUM
eurjchem-336	377	7	4	4	NUM
eurjchem-336	377	8	a	a	DET
eurjchem-336	377	9	yield	yield	NOUN
eurjchem-336	377	10	of	of	ADP
eurjchem-336	377	11	cyclization	cyclization	NOUN
eurjchem-336	377	12	of	of	ADP
eurjchem-336	377	13	3a‐g	3a‐g	NOUN
eurjchem-336	377	14	.	.	PUNCT
eurjchem-336	378	1	b	b	X
eurjchem-336	378	2	yield	yield	NOUN
eurjchem-336	378	3	of	of	ADP
eurjchem-336	378	4	cyclization	cyclization	NOUN
eurjchem-336	378	5	of	of	ADP
eurjchem-336	378	6	4a‐g	4a‐g	NOUN
eurjchem-336	378	7	.	.	PUNCT
eurjchem-336	379	1	on	on	ADP
eurjchem-336	379	2	the	the	DET
eurjchem-336	379	3	other	other	ADJ
eurjchem-336	379	4	hand	hand	NOUN
eurjchem-336	379	5	the	the	DET
eurjchem-336	379	6	excess	excess	NOUN
eurjchem-336	379	7	in	in	ADP
eurjchem-336	379	8	mol%	mol%	PROPN
eurjchem-336	379	9	of	of	ADP
eurjchem-336	379	10	iodine	iodine	NOUN
eurjchem-336	379	11	(	(	PUNCT
eurjchem-336	379	12	1.2	1.2	NUM
eurjchem-336	379	13	equiv	equiv	NOUN
eurjchem-336	379	14	.	.	PUNCT
eurjchem-336	379	15	)	)	PUNCT
eurjchem-336	380	1	on	on	ADP
eurjchem-336	380	2	the	the	DET
eurjchem-336	380	3	mono	mono	NOUN
eurjchem-336	380	4	substituted	substitute	VERB
eurjchem-336	380	5	compounds	compound	NOUN
eurjchem-336	380	6	of	of	ADP
eurjchem-336	380	7	3a‐g	3a‐g	PROPN
eurjchem-336	380	8	&	&	CCONJ
eurjchem-336	380	9	4a‐g	4a‐g	PROPN
eurjchem-336	380	10	leads	lead	VERB
eurjchem-336	380	11	to	to	ADP
eurjchem-336	380	12	iodination	iodination	NOUN
eurjchem-336	380	13	at	at	ADP
eurjchem-336	380	14	the	the	DET
eurjchem-336	380	15	phenol	phenol	NOUN
eurjchem-336	380	16	ring	ring	NOUN
eurjchem-336	380	17	(	(	PUNCT
eurjchem-336	380	18	entry	entry	NOUN
eurjchem-336	380	19	6a	6a	NOUN
eurjchem-336	380	20	,	,	PUNCT
eurjchem-336	380	21	6b	6b	NOUN
eurjchem-336	380	22	and	and	CCONJ
eurjchem-336	380	23	6c	6c	NOUN
eurjchem-336	380	24	,	,	PUNCT
eurjchem-336	380	25	table	table	NOUN
eurjchem-336	380	26	2	2	NUM
eurjchem-336	380	27	,	,	PUNCT
eurjchem-336	380	28	scheme	scheme	NOUN
eurjchem-336	380	29	3	3	NUM
eurjchem-336	380	30	)	)	PUNCT
eurjchem-336	380	31	.	.	PUNCT
eurjchem-336	381	1	if	if	SCONJ
eurjchem-336	381	2	the	the	DET
eurjchem-336	381	3	para	para	NOUN
eurjchem-336	381	4	position	position	NOUN
eurjchem-336	381	5	in	in	ADP
eurjchem-336	381	6	the	the	DET
eurjchem-336	381	7	phenol	phenol	ADJ
eurjchem-336	381	8	moiety	moiety	NOUN
eurjchem-336	381	9	is	be	AUX
eurjchem-336	381	10	blocked	block	VERB
eurjchem-336	381	11	the	the	DET
eurjchem-336	381	12	iodination	iodination	NOUN
eurjchem-336	381	13	takes	take	VERB
eurjchem-336	381	14	place	place	NOUN
eurjchem-336	381	15	at	at	ADP
eurjchem-336	381	16	the	the	DET
eurjchem-336	381	17	ortho	ortho	PROPN
eurjchem-336	381	18	position	position	NOUN
eurjchem-336	381	19	(	(	PUNCT
eurjchem-336	381	20	entry	entry	NOUN
eurjchem-336	381	21	6a	6a	NOUN
eurjchem-336	381	22	,	,	PUNCT
eurjchem-336	381	23	6b	6b	NOUN
eurjchem-336	381	24	,	,	PUNCT
eurjchem-336	381	25	table	table	NOUN
eurjchem-336	381	26	2	2	NUM
eurjchem-336	381	27	)	)	PUNCT
eurjchem-336	381	28	,	,	PUNCT
eurjchem-336	381	29	while	while	SCONJ
eurjchem-336	381	30	if	if	SCONJ
eurjchem-336	381	31	the	the	DET
eurjchem-336	381	32	ortho	ortho	PROPN
eurjchem-336	381	33	position	position	NOUN
eurjchem-336	381	34	is	be	AUX
eurjchem-336	381	35	blocked	block	VERB
eurjchem-336	381	36	the	the	DET
eurjchem-336	381	37	iodination	iodination	NOUN
eurjchem-336	381	38	takes	take	VERB
eurjchem-336	381	39	place	place	NOUN
eurjchem-336	381	40	at	at	ADP
eurjchem-336	381	41	the	the	DET
eurjchem-336	381	42	para	para	NOUN
eurjchem-336	381	43	position	position	NOUN
eurjchem-336	381	44	(	(	PUNCT
eurjchem-336	381	45	entry	entry	NOUN
eurjchem-336	381	46	6c	6c	NOUN
eurjchem-336	381	47	,	,	PUNCT
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eurjchem-336	381	49	2	2	NUM
eurjchem-336	381	50	)	)	PUNCT
eurjchem-336	381	51	.	.	PUNCT
eurjchem-336	382	1	the	the	DET
eurjchem-336	382	2	structure	structure	NOUN
eurjchem-336	382	3	of	of	ADP
eurjchem-336	382	4	the	the	DET
eurjchem-336	382	5	synthesized	synthesize	VERB
eurjchem-336	382	6	compounds	compound	NOUN
eurjchem-336	382	7	was	be	AUX
eurjchem-336	382	8	confirmed	confirm	VERB
eurjchem-336	382	9	on	on	ADP
eurjchem-336	382	10	the	the	DET
eurjchem-336	382	11	basis	basis	NOUN
eurjchem-336	382	12	of	of	ADP
eurjchem-336	382	13	spectroscopic	spectroscopic	ADJ
eurjchem-336	382	14	methods	method	NOUN
eurjchem-336	382	15	.	.	PUNCT
eurjchem-336	383	1	lower	low	ADJ
eurjchem-336	383	2	amount	amount	NOUN
eurjchem-336	383	3	of	of	ADP
eurjchem-336	383	4	iodine	iodine	NOUN
eurjchem-336	383	5	(	(	PUNCT
eurjchem-336	383	6	30	30	NUM
eurjchem-336	383	7	%	%	NOUN
eurjchem-336	383	8	,	,	PUNCT
eurjchem-336	383	9	50	50	NUM
eurjchem-336	383	10	%	%	NOUN
eurjchem-336	383	11	)	)	PUNCT
eurjchem-336	383	12	gave	give	VERB
eurjchem-336	383	13	the	the	DET
eurjchem-336	383	14	mixture	mixture	NOUN
eurjchem-336	383	15	of	of	ADP
eurjchem-336	383	16	iodosubstituted	iodosubstitute	VERB
eurjchem-336	383	17	and	and	CCONJ
eurjchem-336	383	18	unsubstituted	unsubstituted	ADJ
eurjchem-336	383	19	products	product	NOUN
eurjchem-336	383	20	.	.	PUNCT
eurjchem-336	384	1	while	while	SCONJ
eurjchem-336	384	2	in	in	ADP
eurjchem-336	384	3	other	other	ADJ
eurjchem-336	384	4	prazoles	prazole	NOUN
eurjchem-336	384	5	were	be	AUX
eurjchem-336	384	6	already	already	ADV
eurjchem-336	384	7	substituted	substitute	VERB
eurjchem-336	384	8	at	at	ADP
eurjchem-336	384	9	both	both	DET
eurjchem-336	384	10	positions	position	NOUN
eurjchem-336	384	11	in	in	ADP
eurjchem-336	384	12	the	the	DET
eurjchem-336	384	13	phenol	phenol	ADJ
eurjchem-336	384	14	moiety	moiety	NOUN
eurjchem-336	384	15	hence	hence	ADV
eurjchem-336	384	16	no	no	DET
eurjchem-336	384	17	iodination	iodination	NOUN
eurjchem-336	384	18	observed	observe	VERB
eurjchem-336	384	19	.	.	PUNCT
eurjchem-336	385	1	4	4	X
eurjchem-336	385	2	.	.	X
eurjchem-336	385	3	conclusion	conclusion	NOUN
eurjchem-336	385	4	in	in	ADP
eurjchem-336	385	5	summary	summary	NOUN
eurjchem-336	385	6	,	,	PUNCT
eurjchem-336	385	7	we	we	PRON
eurjchem-336	385	8	have	have	AUX
eurjchem-336	385	9	developed	develop	VERB
eurjchem-336	385	10	a	a	DET
eurjchem-336	385	11	simple	simple	ADJ
eurjchem-336	385	12	and	and	CCONJ
eurjchem-336	385	13	convenient	convenient	ADJ
eurjchem-336	385	14	method	method	NOUN
eurjchem-336	385	15	for	for	ADP
eurjchem-336	385	16	the	the	DET
eurjchem-336	385	17	synthesis	synthesis	NOUN
eurjchem-336	385	18	of	of	ADP
eurjchem-336	385	19	2‐arylpyrazolo[4,3‐c]coumarins	2‐arylpyrazolo[4,3‐c]coumarins	NUM
eurjchem-336	385	20	using	use	VERB
eurjchem-336	385	21	i2	i2	NOUN
eurjchem-336	385	22	/	/	SYM
eurjchem-336	385	23	dmso	dmso	NOUN
eurjchem-336	385	24	as	as	ADP
eurjchem-336	385	25	an	an	DET
eurjchem-336	385	26	efficient	efficient	ADJ
eurjchem-336	385	27	catalytic	catalytic	ADJ
eurjchem-336	385	28	system	system	NOUN
eurjchem-336	385	29	.	.	PUNCT
eurjchem-336	386	1	the	the	DET
eurjchem-336	386	2	present	present	ADJ
eurjchem-336	386	3	methodology	methodology	NOUN
eurjchem-336	386	4	is	be	AUX
eurjchem-336	386	5	clean	clean	ADJ
eurjchem-336	386	6	;	;	PUNCT
eurjchem-336	386	7	eliminates	eliminate	VERB
eurjchem-336	386	8	the	the	DET
eurjchem-336	386	9	toxic	toxic	ADJ
eurjchem-336	386	10	metal	metal	NOUN
eurjchem-336	386	11	oxidant	oxidant	NOUN
eurjchem-336	386	12	,	,	PUNCT
eurjchem-336	386	13	228	228	NUM
eurjchem-336	386	14	lokhande	lokhande	VERB
eurjchem-336	386	15	et	et	PROPN
eurjchem-336	386	16	al	al	PROPN
eurjchem-336	386	17	.	.	PUNCT
eurjchem-336	386	18	/	/	SYM
eurjchem-336	386	19	european	european	PROPN
eurjchem-336	386	20	journal	journal	PROPN
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eurjchem-336	386	24	(	(	PUNCT
eurjchem-336	386	25	2	2	NUM
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eurjchem-336	386	27	(	(	PUNCT
eurjchem-336	386	28	2011	2011	NUM
eurjchem-336	386	29	)	)	PUNCT
eurjchem-336	386	30	223‐228	223‐228	NUM
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eurjchem-336	386	32	reaction	reaction	NOUN
eurjchem-336	386	33	times	time	NOUN
eurjchem-336	386	34	,	,	PUNCT
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eurjchem-336	386	37	,	,	PUNCT
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eurjchem-336	386	39	of	of	ADP
eurjchem-336	386	40	workup	workup	NOUN
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eurjchem-336	386	42	more	more	ADV
eurjchem-336	386	43	applicable	applicable	ADJ
eurjchem-336	386	44	for	for	ADP
eurjchem-336	386	45	the	the	DET
eurjchem-336	386	46	medicinal	medicinal	ADJ
eurjchem-336	386	47	as	as	ADV
eurjchem-336	386	48	well	well	ADV
eurjchem-336	386	49	as	as	ADP
eurjchem-336	386	50	pharmaceutical	pharmaceutical	ADJ
eurjchem-336	386	51	chemist	chemist	NOUN
eurjchem-336	386	52	.	.	PUNCT
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eurjchem-336	388	3	(	(	PUNCT
eurjchem-336	388	4	bsr	bsr	NOUN
eurjchem-336	388	5	)	)	PUNCT
eurjchem-336	388	6	]	]	PUNCT
eurjchem-336	388	7	,	,	PUNCT
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eurjchem-336	388	13	.	.	PUNCT
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eurjchem-336	393	1	[	[	X
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eurjchem-336	393	4	.	.	PUNCT
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eurjchem-336	397	2	.	.	PUNCT
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eurjchem-336	398	2	,	,	PUNCT
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eurjchem-336	399	1	[	[	X
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eurjchem-336	403	4	.	.	PUNCT
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eurjchem-336	407	2	,	,	PUNCT
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eurjchem-336	408	1	[	[	X
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eurjchem-336	411	2	.	.	PUNCT
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eurjchem-336	414	2	,	,	PUNCT
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eurjchem-336	415	4	.	.	PUNCT
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eurjchem-336	419	2	,	,	PUNCT
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eurjchem-336	422	2	,	,	PUNCT
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eurjchem-336	427	4	.	.	PUNCT
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eurjchem-336	428	22	.	.	PUNCT
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eurjchem-336	430	2	.	.	PUNCT
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eurjchem-336	431	2	,	,	PUNCT
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eurjchem-336	431	4	,	,	PUNCT
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eurjchem-336	433	22	.	.	PUNCT
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eurjchem-336	434	4	.	.	PUNCT
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eurjchem-336	435	2	,	,	PUNCT
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eurjchem-336	435	4	,	,	PUNCT
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eurjchem-336	437	22	.	.	PUNCT
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eurjchem-336	438	2	.	.	PUNCT
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eurjchem-336	439	2	,	,	PUNCT
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eurjchem-336	440	4	.	.	PUNCT
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eurjchem-336	444	2	.	.	PUNCT
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eurjchem-336	445	2	,	,	PUNCT
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eurjchem-336	449	2	.	.	PUNCT
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eurjchem-336	450	2	,	,	PUNCT
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eurjchem-336	453	2	,	,	PUNCT
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eurjchem-336	455	5	;	;	PUNCT
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eurjchem-336	456	2	,	,	PUNCT
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eurjchem-336	457	4	.	.	PUNCT
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eurjchem-336	458	24	j.	j.	PROPN
eurjchem-336	458	25	k.	k.	PROPN
eurjchem-336	458	26	;	;	PUNCT
eurjchem-336	458	27	chan	chan	PROPN
eurjchem-336	458	28	,	,	PUNCT
eurjchem-336	458	29	p.	p.	PROPN
eurjchem-336	458	30	w.	w.	PROPN
eurjchem-336	458	31	h.	h.	PROPN
eurjchem-336	458	32	tetrahedron	tetrahedron	PROPN
eurjchem-336	458	33	lett	lett	PROPN
eurjchem-336	458	34	.	.	PUNCT
eurjchem-336	458	35	2008	2008	NUM
eurjchem-336	458	36	,	,	PUNCT
eurjchem-336	458	37	49	49	NUM
eurjchem-336	458	38	,	,	PUNCT
eurjchem-336	458	39	122‐126	122‐126	PROPN
eurjchem-336	458	40	.	.	PUNCT
eurjchem-336	459	1	[	[	X
eurjchem-336	459	2	20	20	NUM
eurjchem-336	459	3	]	]	PUNCT
eurjchem-336	459	4	.	.	PUNCT
eurjchem-336	460	1	srihari	srihari	PROPN
eurjchem-336	460	2	,	,	PUNCT
eurjchem-336	460	3	p.	p.	PROPN
eurjchem-336	460	4	;	;	PUNCT
eurjchem-336	460	5	dinesh	dinesh	PROPN
eurjchem-336	460	6	,	,	PUNCT
eurjchem-336	460	7	c.	c.	PROPN
eurjchem-336	460	8	;	;	PUNCT
eurjchem-336	460	9	bhunia	bhunia	NOUN
eurjchem-336	460	10	,	,	PUNCT
eurjchem-336	460	11	p.	p.	NOUN
eurjchem-336	460	12	;	;	PUNCT
eurjchem-336	460	13	sreedhar	sreedhar	PROPN
eurjchem-336	460	14	,	,	PUNCT
eurjchem-336	460	15	s.	s.	PROPN
eurjchem-336	460	16	s.	s.	PROPN
eurjchem-336	460	17	;	;	PUNCT
eurjchem-336	460	18	mandal	mandal	PROPN
eurjchem-336	460	19	,	,	PUNCT
eurjchem-336	460	20	j.	j.	PROPN
eurjchem-336	460	21	;	;	PUNCT
eurjchem-336	460	22	reddy	reddy	PROPN
eurjchem-336	460	23	,	,	PUNCT
eurjchem-336	460	24	j.	j.	PROPN
eurjchem-336	460	25	s.	s.	PROPN
eurjchem-336	460	26	s.	s.	PROPN
eurjchem-336	460	27	;	;	PUNCT
eurjchem-336	460	28	yadav	yadav	PROPN
eurjchem-336	460	29	,	,	PUNCT
eurjchem-336	460	30	j.	j.	PROPN
eurjchem-336	460	31	s.	s.	PROPN
eurjchem-336	460	32	tetrahedron	tetrahedron	PROPN
eurjchem-336	460	33	lett	lett	PROPN
eurjchem-336	460	34	.	.	PUNCT
eurjchem-336	461	1	2007	2007	NUM
eurjchem-336	461	2	,	,	PUNCT
eurjchem-336	461	3	48	48	NUM
eurjchem-336	461	4	,	,	PUNCT
eurjchem-336	461	5	8120‐8124	8120‐8124	NUM
eurjchem-336	461	6	.	.	PUNCT
eurjchem-336	462	1	[	[	X
eurjchem-336	462	2	21	21	NUM
eurjchem-336	462	3	]	]	PUNCT
eurjchem-336	462	4	.	.	PUNCT
eurjchem-336	462	5	sun	sun	PROPN
eurjchem-336	462	6	,	,	PUNCT
eurjchem-336	462	7	g.	g.	PROPN
eurjchem-336	462	8	;	;	PUNCT
eurjchem-336	462	9	wang	wang	PROPN
eurjchem-336	462	10	,	,	PUNCT
eurjchem-336	462	11	z.	z.	PROPN
eurjchem-336	462	12	tetrahedron	tetrahedron	PROPN
eurjchem-336	462	13	lett	lett	PROPN
eurjchem-336	462	14	.	.	PUNCT
eurjchem-336	462	15	2008	2008	NUM
eurjchem-336	462	16	,	,	PUNCT
eurjchem-336	462	17	49	49	NUM
eurjchem-336	462	18	,	,	PUNCT
eurjchem-336	462	19	4929‐4932	4929‐4932	NUM
eurjchem-336	462	20	.	.	PUNCT
eurjchem-336	463	1	[	[	X
eurjchem-336	463	2	22	22	NUM
eurjchem-336	463	3	]	]	PUNCT
eurjchem-336	463	4	.	.	PUNCT
eurjchem-336	464	1	wang	wang	PROPN
eurjchem-336	464	2	,	,	PUNCT
eurjchem-336	464	3	x‐s	x‐s	PROPN
eurjchem-336	464	4	.	.	PUNCT
eurjchem-336	464	5	;	;	PUNCT
eurjchem-336	464	6	zhou	zhou	PROPN
eurjchem-336	464	7	,	,	PUNCT
eurjchem-336	464	8	j.	j.	PROPN
eurjchem-336	464	9	;	;	PUNCT
eurjchem-336	464	10	yin	yin	PROPN
eurjchem-336	464	11	,	,	PUNCT
eurjchem-336	464	12	m.	m.	NOUN
eurjchem-336	464	13	y.	y.	PROPN
eurjchem-336	464	14	;	;	PUNCT
eurjchem-336	464	15	yang	yang	PROPN
eurjchem-336	464	16	,	,	PUNCT
eurjchem-336	464	17	k.	k.	PROPN
eurjchem-336	464	18	;	;	PUNCT
eurjchem-336	464	19	tu	tu	PROPN
eurjchem-336	464	20	.	.	PUNCT
eurjchem-336	464	21	s.	s.	PROPN
eurjchem-336	464	22	j.	j.	PROPN
eurjchem-336	464	23	j.	j.	PROPN
eurjchem-336	464	24	comb	comb	PROPN
eurjchem-336	464	25	.	.	PUNCT
eurjchem-336	465	1	chem	chem	NOUN
eurjchem-336	465	2	.	.	PUNCT
eurjchem-336	466	1	2010	2010	NUM
eurjchem-336	466	2	,	,	PUNCT
eurjchem-336	466	3	12	12	NUM
eurjchem-336	466	4	,	,	PUNCT
eurjchem-336	466	5	266‐269	266‐269	NUM
eurjchem-336	466	6	.	.	PUNCT
eurjchem-336	467	1	[	[	X
eurjchem-336	467	2	23	23	NUM
eurjchem-336	467	3	]	]	PUNCT
eurjchem-336	467	4	.	.	PUNCT
eurjchem-336	468	1	lin	lin	PROPN
eurjchem-336	468	2	,	,	PUNCT
eurjchem-336	468	3	x.	x.	PROPN
eurjchem-336	468	4	f.	f.	PROPN
eurjchem-336	468	5	;	;	PUNCT
eurjchem-336	468	6	cui	cui	PROPN
eurjchem-336	468	7	,	,	PUNCT
eurjchem-336	468	8	s.	s.	PROPN
eurjchem-336	468	9	l.	l.	PROPN
eurjchem-336	468	10	;	;	PUNCT
eurjchem-336	468	11	wang	wang	PROPN
eurjchem-336	468	12	,	,	PUNCT
eurjchem-336	468	13	y.	y.	PROPN
eurjchem-336	468	14	g.	g.	PROPN
eurjchem-336	468	15	tetrahedron	tetrahedron	PROPN
eurjchem-336	468	16	lett	lett	PROPN
eurjchem-336	468	17	.	.	PUNCT
eurjchem-336	469	1	2006	2006	NUM
eurjchem-336	469	2	,	,	PUNCT
eurjchem-336	469	3	47	47	NUM
eurjchem-336	469	4	,	,	PUNCT
eurjchem-336	469	5	4509‐4512	4509‐4512	NOUN
eurjchem-336	469	6	.	.	PUNCT
eurjchem-336	470	1	[	[	X
eurjchem-336	470	2	24	24	NUM
eurjchem-336	470	3	]	]	PUNCT
eurjchem-336	470	4	.	.	PUNCT
eurjchem-336	471	1	lin	lin	PROPN
eurjchem-336	471	2	,	,	PUNCT
eurjchem-336	471	3	x.	x.	PROPN
eurjchem-336	471	4	;	;	PUNCT
eurjchem-336	471	5	dai	dai	PROPN
eurjchem-336	471	6	,	,	PUNCT
eurjchem-336	471	7	x.	x.	PROPN
eurjchem-336	471	8	;	;	PUNCT
eurjchem-336	471	9	mao	mao	PROPN
eurjchem-336	471	10	,	,	PUNCT
eurjchem-336	471	11	z.	z.	PROPN
eurjchem-336	471	12	;	;	PUNCT
eurjchem-336	471	13	wang	wang	PROPN
eurjchem-336	471	14	,	,	PUNCT
eurjchem-336	471	15	y.	y.	PROPN
eurjchem-336	471	16	tetrahedron	tetrahedron	PROPN
eurjchem-336	471	17	2009	2009	NUM
eurjchem-336	471	18	,	,	PUNCT
eurjchem-336	471	19	65	65	NUM
eurjchem-336	471	20	,	,	PUNCT
eurjchem-336	471	21	9233‐9237	9233‐9237	NUM
eurjchem-336	471	22	.	.	PUNCT
eurjchem-336	472	1	[	[	X
eurjchem-336	472	2	25	25	NUM
eurjchem-336	472	3	]	]	PUNCT
eurjchem-336	472	4	.	.	PUNCT
eurjchem-336	473	1	zmitek	zmitek	PROPN
eurjchem-336	473	2	,	,	PUNCT
eurjchem-336	473	3	k.	k.	PROPN
eurjchem-336	473	4	;	;	PUNCT
eurjchem-336	473	5	zupan	zupan	NOUN
eurjchem-336	473	6	,	,	PUNCT
eurjchem-336	473	7	m.	m.	NOUN
eurjchem-336	473	8	;	;	PUNCT
eurjchem-336	473	9	stavber	stavber	PROPN
eurjchem-336	473	10	,	,	PUNCT
eurjchem-336	473	11	s.	s.	PROPN
eurjchem-336	473	12	;	;	PUNCT
eurjchem-336	473	13	iskra	iskra	PROPN
eurjchem-336	473	14	,	,	PUNCT
eurjchem-336	473	15	j.	j.	PROPN
eurjchem-336	473	16	org	org	PROPN
eurjchem-336	473	17	.	.	PUNCT
eurjchem-336	474	1	lett	lett	PROPN
eurjchem-336	474	2	.	.	PUNCT
eurjchem-336	475	1	2006	2006	NUM
eurjchem-336	475	2	,	,	PUNCT
eurjchem-336	475	3	8	8	NUM
eurjchem-336	475	4	,	,	PUNCT
eurjchem-336	475	5	2491‐	2491‐	NUM
eurjchem-336	475	6	2494	2494	NUM
eurjchem-336	475	7	.	.	PUNCT
eurjchem-336	476	1	[	[	X
eurjchem-336	476	2	26	26	NUM
eurjchem-336	476	3	]	]	PUNCT
eurjchem-336	476	4	.	.	PUNCT
eurjchem-336	477	1	wang	wang	PROPN
eurjchem-336	477	2	,	,	PUNCT
eurjchem-336	477	3	j.	j.	PROPN
eurjchem-336	477	4	;	;	PUNCT
eurjchem-336	477	5	xu	xu	PROPN
eurjchem-336	477	6	,	,	PUNCT
eurjchem-336	477	7	f.	f.	PROPN
eurjchem-336	477	8	x.	x.	PROPN
eurjchem-336	477	9	;	;	PUNCT
eurjchem-336	477	10	lin	lin	PROPN
eurjchem-336	477	11	,	,	PUNCT
eurjchem-336	477	12	x.	x.	PROPN
eurjchem-336	477	13	f.	f.	PROPN
eurjchem-336	477	14	;	;	PUNCT
eurjchem-336	477	15	wang	wang	PROPN
eurjchem-336	477	16	,	,	PUNCT
eurjchem-336	477	17	y.	y.	PROPN
eurjchem-336	477	18	g.	g.	PROPN
eurjchem-336	477	19	tetrahedron	tetrahedron	PROPN
eurjchem-336	477	20	lett	lett	PROPN
eurjchem-336	477	21	.	.	PUNCT
eurjchem-336	477	22	2008	2008	NUM
eurjchem-336	477	23	,	,	PUNCT
eurjchem-336	477	24	49	49	NUM
eurjchem-336	477	25	,	,	PUNCT
eurjchem-336	477	26	5208‐5210	5208‐5210	NUM
eurjchem-336	477	27	.	.	PUNCT
eurjchem-336	478	1	[	[	X
eurjchem-336	478	2	27	27	NUM
eurjchem-336	478	3	]	]	PUNCT
eurjchem-336	478	4	.	.	PUNCT
eurjchem-336	479	1	lin	lin	PROPN
eurjchem-336	479	2	,	,	PUNCT
eurjchem-336	479	3	x.	x.	PROPN
eurjchem-336	479	4	f.	f.	PROPN
eurjchem-336	479	5	;	;	PUNCT
eurjchem-336	479	6	cui	cui	PROPN
eurjchem-336	479	7	,	,	PUNCT
eurjchem-336	479	8	s.	s.	PROPN
eurjchem-336	479	9	l.	l.	PROPN
eurjchem-336	479	10	;	;	PUNCT
eurjchem-336	479	11	wang	wang	PROPN
eurjchem-336	479	12	,	,	PUNCT
eurjchem-336	479	13	y.	y.	PROPN
eurjchem-336	479	14	g.	g.	PROPN
eurjchem-336	479	15	tetrahedron	tetrahedron	PROPN
eurjchem-336	479	16	lett	lett	PROPN
eurjchem-336	479	17	.	.	PUNCT
eurjchem-336	480	1	2006	2006	NUM
eurjchem-336	480	2	,	,	PUNCT
eurjchem-336	480	3	47	47	NUM
eurjchem-336	480	4	,	,	PUNCT
eurjchem-336	480	5	3127‐3130	3127‐3130	NUM
eurjchem-336	480	6	.	.	PUNCT
eurjchem-336	481	1	[	[	X
eurjchem-336	481	2	28	28	NUM
eurjchem-336	481	3	]	]	PUNCT
eurjchem-336	481	4	.	.	PUNCT
eurjchem-336	482	1	sun	sun	PROPN
eurjchem-336	482	2	,	,	PUNCT
eurjchem-336	482	3	j.	j.	PROPN
eurjchem-336	482	4	;	;	PUNCT
eurjchem-336	482	5	dong	dong	PROPN
eurjchem-336	482	6	,	,	PUNCT
eurjchem-336	482	7	y.	y.	PROPN
eurjchem-336	482	8	;	;	PUNCT
eurjchem-336	482	9	cao	cao	PROPN
eurjchem-336	482	10	,	,	PUNCT
eurjchem-336	482	11	l.	l.	PROPN
eurjchem-336	482	12	;	;	PUNCT
eurjchem-336	482	13	wang	wang	PROPN
eurjchem-336	482	14	,	,	PUNCT
eurjchem-336	482	15	x.	x.	PROPN
eurjchem-336	482	16	;	;	PUNCT
eurjchem-336	482	17	wang	wang	PROPN
eurjchem-336	482	18	,	,	PUNCT
eurjchem-336	482	19	s.	s.	PROPN
eurjchem-336	482	20	;	;	PUNCT
eurjchem-336	482	21	hu	hu	PROPN
eurjchem-336	482	22	,	,	PUNCT
eurjchem-336	482	23	y.	y.	PROPN
eurjchem-336	482	24	j.	j.	PROPN
eurjchem-336	482	25	org	org	PROPN
eurjchem-336	482	26	.	.	PUNCT
eurjchem-336	482	27	chem	chem	PROPN
eurjchem-336	482	28	.	.	PUNCT
eurjchem-336	483	1	2004	2004	NUM
eurjchem-336	483	2	,	,	PUNCT
eurjchem-336	483	3	69	69	NUM
eurjchem-336	483	4	,	,	PUNCT
eurjchem-336	483	5	8932‐8934	8932‐8934	ADJ
eurjchem-336	483	6	.	.	PUNCT
eurjchem-336	484	1	[	[	X
eurjchem-336	484	2	29	29	NUM
eurjchem-336	484	3	]	]	PUNCT
eurjchem-336	484	4	.	.	PUNCT
eurjchem-336	484	5	lokhande	lokhande	PROPN
eurjchem-336	484	6	,	,	PUNCT
eurjchem-336	484	7	p.	p.	PROPN
eurjchem-336	484	8	d.	d.	PROPN
eurjchem-336	484	9	;	;	PUNCT
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eurjchem-336	484	11	b.	b.	PROPN
eurjchem-336	484	12	y.	y.	PROPN
eurjchem-336	484	13	;	;	PUNCT
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eurjchem-336	484	16	s.	s.	PROPN
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eurjchem-336	484	18	j.	j.	PROPN
eurjchem-336	484	19	chem	chem	PROPN
eurjchem-336	484	20	,	,	PUNCT
eurjchem-336	484	21	2005	2005	NUM
eurjchem-336	484	22	,	,	PUNCT
eurjchem-336	484	23	44b	44b	NUM
eurjchem-336	484	24	,	,	PUNCT
eurjchem-336	484	25	2338‐2342	2338‐2342	NUM
eurjchem-336	484	26	.	.	PUNCT
eurjchem-336	485	1	[	[	X
eurjchem-336	485	2	30	30	NUM
eurjchem-336	485	3	]	]	PUNCT
eurjchem-336	485	4	.	.	PUNCT
eurjchem-336	486	1	lokhande	lokhande	PROPN
eurjchem-336	486	2	,	,	PUNCT
eurjchem-336	486	3	p.	p.	PROPN
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eurjchem-336	486	5	;	;	PUNCT
eurjchem-336	486	6	sakte	sakte	PROPN
eurjchem-336	486	7	,	,	PUNCT
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eurjchem-336	486	9	,	,	PUNCT
eurjchem-336	486	10	s.	s.	PROPN
eurjchem-336	486	11	;	;	PUNCT
eurjchem-336	486	12	taksande	taksande	PROPN
eurjchem-336	486	13	k	k	PROPN
eurjchem-336	486	14	,	,	PUNCT
eurjchem-336	486	15	n.	n.	NOUN
eurjchem-336	486	16	;	;	PUNCT
eurjchem-336	486	17	navghare	navghare	NOUN
eurjchem-336	486	18	,	,	PUNCT
eurjchem-336	486	19	b.	b.	PROPN
eurjchem-336	486	20	tetrahedron	tetrahedron	PROPN
eurjchem-336	486	21	lett	lett	PROPN
eurjchem-336	486	22	.	.	PUNCT
eurjchem-336	487	1	2005	2005	NUM
eurjchem-336	487	2	,	,	PUNCT
eurjchem-336	487	3	46	46	NUM
eurjchem-336	487	4	,	,	PUNCT
eurjchem-336	487	5	1573‐1574	1573‐1574	NUM
eurjchem-336	487	6	.	.	PUNCT
eurjchem-336	488	1	[	[	X
eurjchem-336	488	2	31	31	NUM
eurjchem-336	488	3	]	]	PUNCT
eurjchem-336	488	4	.	.	PUNCT
eurjchem-336	488	5	lokhande	lokhande	PROPN
eurjchem-336	488	6	,	,	PUNCT
eurjchem-336	488	7	p.	p.	PROPN
eurjchem-336	488	8	d.	d.	PROPN
eurjchem-336	488	9	;	;	PUNCT
eurjchem-336	488	10	ghiya	ghiya	PROPN
eurjchem-336	488	11	b.	b.	PROPN
eurjchem-336	488	12	j.	j.	PROPN
eurjchem-336	488	13	j.	j.	PROPN
eurjchem-336	488	14	indian	indian	PROPN
eurjchem-336	488	15	chem	chem	PROPN
eurjchem-336	488	16	.	.	PUNCT
eurjchem-336	489	1	soc	soc	PROPN
eurjchem-336	489	2	.	.	PUNCT
eurjchem-336	490	1	1991	1991	NUM
eurjchem-336	490	2	,	,	PUNCT
eurjchem-336	490	3	68	68	NUM
eurjchem-336	490	4	,	,	PUNCT
eurjchem-336	490	5	412‐413	412‐413	PROPN
eurjchem-336	490	6	.	.	PUNCT
eurjchem-336	491	1	[	[	X
eurjchem-336	491	2	32	32	NUM
eurjchem-336	491	3	]	]	PUNCT
eurjchem-336	491	4	.	.	PUNCT
eurjchem-336	492	1	vogel	vogel	PROPN
eurjchem-336	492	2	's	's	PART
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eurjchem-336	492	4	book	book	NOUN
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eurjchem-336	492	8	,	,	PUNCT
eurjchem-336	492	9	5th	5th	ADJ
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eurjchem-336	492	11	,	,	PUNCT
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eurjchem-336	492	13	,	,	PUNCT
eurjchem-336	492	14	london	london	PROPN
eurjchem-336	492	15	,	,	PUNCT
eurjchem-336	492	16	1989	1989	NUM
eurjchem-336	492	17	.	.	PUNCT
eurjchem-336	493	1	[	[	X
eurjchem-336	493	2	33	33	NUM
eurjchem-336	493	3	]	]	PUNCT
eurjchem-336	493	4	.	.	PUNCT
eurjchem-336	493	5	alkhathlan	alkhathlan	PROPN
eurjchem-336	493	6	,	,	PUNCT
eurjchem-336	493	7	h.	h.	PROPN
eurjchem-336	493	8	z.	z.	PROPN
eurjchem-336	493	9	tetrahedron	tetrahedron	PROPN
eurjchem-336	493	10	,	,	PUNCT
eurjchem-336	493	11	2003	2003	NUM
eurjchem-336	493	12	,	,	PUNCT
eurjchem-336	493	13	59	59	NUM
eurjchem-336	493	14	,	,	PUNCT
eurjchem-336	493	15	8163‐8170	8163‐8170	NUM
eurjchem-336	493	16	.	.	PUNCT
eurjchem-336	494	1	[	[	X
eurjchem-336	494	2	34	34	NUM
eurjchem-336	494	3	]	]	PUNCT
eurjchem-336	494	4	.	.	PUNCT
eurjchem-336	495	1	rathelot	rathelot	NOUN
eurjchem-336	495	2	,	,	PUNCT
eurjchem-336	495	3	p.	p.	NOUN
eurjchem-336	495	4	;	;	PUNCT
eurjchem-336	495	5	azas	aza	NOUN
eurjchem-336	495	6	,	,	PUNCT
eurjchem-336	495	7	n.	n.	NOUN
eurjchem-336	495	8	;	;	PUNCT
eurjchem-336	495	9	kashef	kashef	PROPN
eurjchem-336	495	10	,	,	PUNCT
eurjchem-336	495	11	h.	h.	PROPN
eurjchem-336	495	12	e.	e.	PROPN
eurjchem-336	495	13	;	;	PUNCT
eurjchem-336	495	14	delmas	delmas	PROPN
eurjchem-336	495	15	,	,	PUNCT
eurjchem-336	495	16	f.	f.	PROPN
eurjchem-336	495	17	;	;	PUNCT
eurjchem-336	495	18	giorgio	giorgio	PROPN
eurjchem-336	495	19	,	,	PUNCT
eurjchem-336	495	20	c.	c.	PROPN
eurjchem-336	495	21	d.	d.	PROPN
eurjchem-336	495	22	;	;	PUNCT
eurjchem-336	495	23	david	david	PROPN
eurjchem-336	495	24	,	,	PUNCT
eurjchem-336	495	25	p.	p.	PROPN
eurjchem-336	495	26	t.	t.	PROPN
eurjchem-336	495	27	;	;	PUNCT
eurjchem-336	495	28	maldonado	maldonado	PROPN
eurjchem-336	495	29	,	,	PUNCT
eurjchem-336	495	30	j.	j.	PROPN
eurjchem-336	495	31	;	;	PUNCT
eurjchem-336	495	32	vanelle	vanelle	NOUN
eurjchem-336	495	33	,	,	PUNCT
eurjchem-336	495	34	p.	p.	PROPN
eurjchem-336	495	35	eur	eur	PROPN
eurjchem-336	495	36	.	.	PUNCT
eurjchem-336	496	1	j.	j.	PROPN
eurjchem-336	496	2	med	med	PROPN
eurjchem-336	496	3	.	.	PROPN
eurjchem-336	496	4	chem	chem	PROPN
eurjchem-336	496	5	.	.	PUNCT
eurjchem-336	497	1	2002	2002	NUM
eurjchem-336	497	2	,	,	PUNCT
eurjchem-336	497	3	37	37	NUM
eurjchem-336	497	4	,	,	PUNCT
eurjchem-336	497	5	671‐679	671‐679	PROPN
eurjchem-336	497	6	.	.	PUNCT