id	sid	tid	token	lemma	pos
eurjchem-365	1	1	untitled	untitle	VERB
eurjchem-365	1	2	european	european	PROPN
eurjchem-365	1	3	journal	journal	PROPN
eurjchem-365	1	4	of	of	ADP
eurjchem-365	1	5	chemistry	chemistry	NOUN
eurjchem-365	1	6	2	2	NUM
eurjchem-365	1	7	(	(	PUNCT
eurjchem-365	1	8	2	2	NUM
eurjchem-365	1	9	)	)	PUNCT
eurjchem-365	1	10	(	(	PUNCT
eurjchem-365	1	11	2011	2011	NUM
eurjchem-365	1	12	)	)	PUNCT
eurjchem-365	1	13	200‐205	200‐205	NUM
eurjchem-365	1	14	european	european	PROPN
eurjchem-365	1	15	journal	journal	PROPN
eurjchem-365	1	16	of	of	ADP
eurjchem-365	1	17	chemistry	chemistry	NOUN
eurjchem-365	1	18	issn	issn	PROPN
eurjchem-365	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-365	1	20	(	(	PUNCT
eurjchem-365	1	21	print	print	NOUN
eurjchem-365	1	22	)	)	PUNCT
eurjchem-365	1	23	/	/	SYM
eurjchem-365	1	24	issn	issn	PROPN
eurjchem-365	1	25	2153‐2257	2153‐2257	NUM
eurjchem-365	1	26	(	(	PUNCT
eurjchem-365	1	27	online	online	ADJ
eurjchem-365	1	28	)	)	PUNCT
eurjchem-365	1	29			NOUN
eurjchem-365	1	30	2011	2011	NUM
eurjchem-365	1	31	eurjchem	eurjchem	PROPN
eurjchem-365	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-365	1	33	/	/	SYM
eurjchem-365	1	34	eurjchem.2.2.200‐205.365	eurjchem.2.2.200‐205.365	PROPN
eurjchem-365	1	35	european	european	PROPN
eurjchem-365	1	36	journal	journal	PROPN
eurjchem-365	1	37	of	of	ADP
eurjchem-365	1	38	chemistry	chemistry	PROPN
eurjchem-365	1	39	journal	journal	PROPN
eurjchem-365	1	40	homepage	homepage	NOUN
eurjchem-365	1	41	:	:	PUNCT
eurjchem-365	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-365	1	43	utility	utility	NOUN
eurjchem-365	1	44	of	of	ADP
eurjchem-365	1	45	2‐cyano‐3‐phenyl‐2‐propenoyl	2‐cyano‐3‐phenyl‐2‐propenoyl	PROPN
eurjchem-365	1	46	chloride	chloride	NOUN
eurjchem-365	1	47	as	as	ADP
eurjchem-365	1	48	michael	michael	PROPN
eurjchem-365	1	49	’s	’s	PART
eurjchem-365	1	50	acceptor	acceptor	NOUN
eurjchem-365	1	51	in	in	ADP
eurjchem-365	1	52	heterocyclic	heterocyclic	ADJ
eurjchem-365	1	53	synthesis	synthesis	NOUN
eurjchem-365	1	54	with	with	ADP
eurjchem-365	1	55	mono‐	mono‐	NOUN
eurjchem-365	1	56	and	and	CCONJ
eurjchem-365	1	57	bi‐dentate	bi‐dentate	ADJ
eurjchem-365	1	58	nucleophiles	nucleophile	NOUN
eurjchem-365	1	59	sayed	say	VERB
eurjchem-365	1	60	ahmed	ahmed	PROPN
eurjchem-365	1	61	shibaa	shibaa	PROPN
eurjchem-365	1	62	,	,	PUNCT
eurjchem-365	1	63	hassan	hassan	PROPN
eurjchem-365	1	64	mohamed	mohamed	PROPN
eurjchem-365	1	65	fawzy	fawzy	PROPN
eurjchem-365	1	66	madkoura	madkoura	PROPN
eurjchem-365	1	67	,	,	PUNCT
eurjchem-365	1	68	b	b	PROPN
eurjchem-365	1	69	,	,	PUNCT
eurjchem-365	1	70	*	*	PUNCT
eurjchem-365	1	71	,	,	PUNCT
eurjchem-365	1	72	ashraf	ashraf	PROPN
eurjchem-365	1	73	ahmed	ahmed	PROPN
eurjchem-365	1	74	hameda	hameda	PROPN
eurjchem-365	1	75	,	,	PUNCT
eurjchem-365	1	76	hatem	hatem	PROPN
eurjchem-365	1	77	mohamed	mohamed	PROPN
eurjchem-365	1	78	sayeda	sayeda	PROPN
eurjchem-365	1	79	and	and	CCONJ
eurjchem-365	1	80	maher	maher	PROPN
eurjchem-365	1	81	abd	abd	PROPN
eurjchem-365	1	82	el‐aziz	el‐aziz	PROPN
eurjchem-365	1	83	el‐hashasha	el‐hashasha	PROPN
eurjchem-365	1	84	a	a	DET
eurjchem-365	1	85	chemistry	chemistry	NOUN
eurjchem-365	1	86	department	department	NOUN
eurjchem-365	1	87	,	,	PUNCT
eurjchem-365	1	88	faculty	faculty	NOUN
eurjchem-365	1	89	of	of	ADP
eurjchem-365	1	90	science	science	NOUN
eurjchem-365	1	91	,	,	PUNCT
eurjchem-365	1	92	ain	ain	PROPN
eurjchem-365	1	93	shams	shams	PROPN
eurjchem-365	1	94	university	university	PROPN
eurjchem-365	1	95	,	,	PUNCT
eurjchem-365	1	96	abbasiya	abbasiya	NOUN
eurjchem-365	1	97	,	,	PUNCT
eurjchem-365	1	98	11566	11566	NUM
eurjchem-365	1	99	,	,	PUNCT
eurjchem-365	1	100	cairo	cairo	PROPN
eurjchem-365	1	101	,	,	PUNCT
eurjchem-365	1	102	egypt	egypt	PROPN
eurjchem-365	1	103	b	b	PROPN
eurjchem-365	1	104	institute	institute	PROPN
eurjchem-365	1	105	of	of	ADP
eurjchem-365	1	106	biochemistry	biochemistry	NOUN
eurjchem-365	1	107	,	,	PUNCT
eurjchem-365	1	108	university	university	NOUN
eurjchem-365	1	109	of	of	ADP
eurjchem-365	1	110	balochistan	balochistan	PROPN
eurjchem-365	1	111	,	,	PUNCT
eurjchem-365	1	112	quetta	quetta	PROPN
eurjchem-365	1	113	,	,	PUNCT
eurjchem-365	1	114	87300	87300	NUM
eurjchem-365	1	115	,	,	PUNCT
eurjchem-365	1	116	pakistan	pakistan	PROPN
eurjchem-365	1	117	*	*	PUNCT
eurjchem-365	1	118	corresponding	correspond	VERB
eurjchem-365	1	119	author	author	NOUN
eurjchem-365	1	120	at	at	ADP
eurjchem-365	1	121	:	:	PUNCT
eurjchem-365	1	122	chemistry	chemistry	NOUN
eurjchem-365	1	123	department	department	NOUN
eurjchem-365	1	124	,	,	PUNCT
eurjchem-365	1	125	faculty	faculty	NOUN
eurjchem-365	1	126	of	of	ADP
eurjchem-365	1	127	science	science	NOUN
eurjchem-365	1	128	,	,	PUNCT
eurjchem-365	1	129	ain	ain	PROPN
eurjchem-365	1	130	shams	shams	PROPN
eurjchem-365	1	131	university	university	PROPN
eurjchem-365	1	132	,	,	PUNCT
eurjchem-365	1	133	abbasiya	abbasiya	NOUN
eurjchem-365	1	134	,	,	PUNCT
eurjchem-365	1	135	11566	11566	NUM
eurjchem-365	1	136	,	,	PUNCT
eurjchem-365	1	137	cairo	cairo	PROPN
eurjchem-365	1	138	,	,	PUNCT
eurjchem-365	1	139	egypt	egypt	PROPN
eurjchem-365	1	140	.	.	PUNCT
eurjchem-365	2	1	tel	tel	PROPN
eurjchem-365	2	2	.	.	PUNCT
eurjchem-365	2	3	:	:	PUNCT
eurjchem-365	3	1	+202.24831836	+202.24831836	X
eurjchem-365	3	2	;	;	PUNCT
eurjchem-365	3	3	fax	fax	NOUN
eurjchem-365	3	4	:	:	PUNCT
eurjchem-365	3	5	+202.24831836	+202.24831836	PROPN
eurjchem-365	3	6	.	.	PUNCT
eurjchem-365	3	7	e‐mail	e‐mail	PUNCT
eurjchem-365	4	1	address	address	NOUN
eurjchem-365	4	2	:	:	PUNCT
eurjchem-365	4	3	fawzy.hassan@ymail.com	fawzy.hassan@ymail.com	X
eurjchem-365	4	4	(	(	PUNCT
eurjchem-365	4	5	h.m.f	h.m.f	PROPN
eurjchem-365	4	6	.	.	PUNCT
eurjchem-365	4	7	madkour	madkour	PROPN
eurjchem-365	4	8	)	)	PUNCT
eurjchem-365	4	9	.	.	PUNCT
eurjchem-365	5	1	article	article	NOUN
eurjchem-365	5	2	information	information	PROPN
eurjchem-365	5	3	abstract	abstract	ADV
eurjchem-365	5	4	received	receive	VERB
eurjchem-365	5	5	:	:	PUNCT
eurjchem-365	5	6	07	07	NUM
eurjchem-365	5	7	december	december	PROPN
eurjchem-365	5	8	2010	2010	NUM
eurjchem-365	5	9	received	receive	VERB
eurjchem-365	5	10	in	in	ADP
eurjchem-365	5	11	revised	revise	VERB
eurjchem-365	5	12	form	form	NOUN
eurjchem-365	5	13	:	:	PUNCT
eurjchem-365	5	14	05	05	NUM
eurjchem-365	5	15	april	april	PROPN
eurjchem-365	5	16	2011	2011	NUM
eurjchem-365	5	17	accepted	accept	VERB
eurjchem-365	5	18	:	:	PUNCT
eurjchem-365	5	19	05	05	NUM
eurjchem-365	5	20	april	april	PROPN
eurjchem-365	5	21	2011	2011	NUM
eurjchem-365	5	22	online	online	ADV
eurjchem-365	5	23	:	:	PUNCT
eurjchem-365	5	24	30	30	NUM
eurjchem-365	5	25	june	june	PROPN
eurjchem-365	5	26	2011	2011	NUM
eurjchem-365	5	27	keywords	keyword	NOUN
eurjchem-365	5	28	(	(	PUNCT
eurjchem-365	5	29	e	e	NOUN
eurjchem-365	5	30	)	)	PUNCT
eurjchem-365	5	31	2‐cyano‐3‐phenyl‐2‐propenoyl	2‐cyano‐3‐phenyl‐2‐propenoyl	PROPN
eurjchem-365	5	32	chloride	chloride	NOUN
eurjchem-365	5	33	reacts	react	NOUN
eurjchem-365	5	34	with	with	ADP
eurjchem-365	5	35	nitrogen	nitrogen	NOUN
eurjchem-365	5	36	,	,	PUNCT
eurjchem-365	5	37	oxygen	oxygen	NOUN
eurjchem-365	5	38	and	and	CCONJ
eurjchem-365	5	39	sulphur	sulphur	NOUN
eurjchem-365	5	40	mono‐	mono‐	NOUN
eurjchem-365	5	41	and	and	CCONJ
eurjchem-365	5	42	bi‐dentate	bi‐dentate	ADJ
eurjchem-365	5	43	nucleophilic	nucleophilic	ADJ
eurjchem-365	5	44	reagents	reagent	NOUN
eurjchem-365	5	45	to	to	PART
eurjchem-365	5	46	give	give	VERB
eurjchem-365	5	47	the	the	DET
eurjchem-365	5	48	amide	amide	NOUN
eurjchem-365	5	49	derivatives	derivative	NOUN
eurjchem-365	5	50	,	,	PUNCT
eurjchem-365	5	51	the	the	DET
eurjchem-365	5	52	ester	ester	NOUN
eurjchem-365	5	53	derivatives	derivative	NOUN
eurjchem-365	5	54	,	,	PUNCT
eurjchem-365	5	55	as	as	ADV
eurjchem-365	5	56	well	well	ADV
eurjchem-365	5	57	as	as	ADP
eurjchem-365	5	58	some	some	DET
eurjchem-365	5	59	heterocyclic	heterocyclic	ADJ
eurjchem-365	5	60	systems	system	NOUN
eurjchem-365	5	61	,	,	PUNCT
eurjchem-365	5	62	namely	namely	ADV
eurjchem-365	5	63	quinazolinone	quinazolinone	NUM
eurjchem-365	5	64	,	,	PUNCT
eurjchem-365	5	65	pyridopyrimidine	pyridopyrimidine	NOUN
eurjchem-365	5	66	and	and	CCONJ
eurjchem-365	5	67	benzothiazepine	benzothiazepine	NOUN
eurjchem-365	5	68	.	.	PUNCT
eurjchem-365	6	1	cyclization	cyclization	NOUN
eurjchem-365	6	2	of	of	ADP
eurjchem-365	6	3	some	some	DET
eurjchem-365	6	4	obtained	obtain	VERB
eurjchem-365	6	5	amides	amide	NOUN
eurjchem-365	6	6	affords	afford	VERB
eurjchem-365	6	7	the	the	DET
eurjchem-365	6	8	benzoxazinones	benzoxazinone	NOUN
eurjchem-365	6	9	,	,	PUNCT
eurjchem-365	6	10	quinazolinone	quinazolinone	NUM
eurjchem-365	6	11	,	,	PUNCT
eurjchem-365	6	12	whereas	whereas	SCONJ
eurjchem-365	6	13	that	that	PRON
eurjchem-365	6	14	of	of	ADP
eurjchem-365	6	15	other	other	ADJ
eurjchem-365	6	16	amides	amide	NOUN
eurjchem-365	6	17	yields	yield	NOUN
eurjchem-365	6	18	oxadiazole	oxadiazole	NOUN
eurjchem-365	6	19	and	and	CCONJ
eurjchem-365	6	20	benzoxazole	benzoxazole	NOUN
eurjchem-365	6	21	,	,	PUNCT
eurjchem-365	6	22	respectively	respectively	ADV
eurjchem-365	6	23	.	.	PUNCT
eurjchem-365	7	1	mono‐	mono‐	NOUN
eurjchem-365	7	2	and	and	CCONJ
eurjchem-365	7	3	bi‐dentate	bi‐dentate	ADJ
eurjchem-365	7	4	nucleophiles	nucleophile	NOUN
eurjchem-365	8	1	2‐propenoyl	2‐propenoyl	PROPN
eurjchem-365	8	2	chloride	chloride	NOUN
eurjchem-365	8	3	benzoxazinone	benzoxazinone	NOUN
eurjchem-365	8	4	quinazolinone	quinazolinone	NOUN
eurjchem-365	8	5	oxadiazole	oxadiazole	NOUN
eurjchem-365	8	6	benzoxazole	benzoxazole	NOUN
eurjchem-365	8	7	1	1	NUM
eurjchem-365	8	8	.	.	PUNCT
eurjchem-365	9	1	introduction	introduction	NOUN
eurjchem-365	9	2	the	the	DET
eurjchem-365	9	3	recent	recent	ADJ
eurjchem-365	9	4	pharmaceutical	pharmaceutical	ADJ
eurjchem-365	9	5	applications	application	NOUN
eurjchem-365	9	6	of	of	ADP
eurjchem-365	9	7	2‐propenoyl	2‐propenoyl	PROPN
eurjchem-365	9	8	amides	amide	NOUN
eurjchem-365	9	9	[	[	X
eurjchem-365	9	10	1	1	NUM
eurjchem-365	9	11	]	]	PUNCT
eurjchem-365	9	12	,	,	PUNCT
eurjchem-365	9	13	2‐propenoates	2‐propenoate	NOUN
eurjchem-365	9	14	[	[	X
eurjchem-365	9	15	2,3	2,3	NUM
eurjchem-365	9	16	]	]	PUNCT
eurjchem-365	9	17	,	,	PUNCT
eurjchem-365	9	18	and	and	CCONJ
eurjchem-365	9	19	other	other	ADJ
eurjchem-365	9	20	heterocyclic	heterocyclic	ADJ
eurjchem-365	9	21	skeletons	skeleton	NOUN
eurjchem-365	9	22	,	,	PUNCT
eurjchem-365	9	23	like	like	ADP
eurjchem-365	9	24	benzoxazinones	benzoxazinone	NOUN
eurjchem-365	9	25	[	[	X
eurjchem-365	9	26	4,5	4,5	NUM
eurjchem-365	9	27	]	]	PUNCT
eurjchem-365	9	28	,	,	PUNCT
eurjchem-365	9	29	quinazolinones	quinazolinone	NOUN
eurjchem-365	9	30	[	[	X
eurjchem-365	9	31	6	6	NUM
eurjchem-365	9	32	]	]	PUNCT
eurjchem-365	9	33	,	,	PUNCT
eurjchem-365	9	34	benzoxazoles	benzoxazole	VERB
eurjchem-365	9	35	[	[	X
eurjchem-365	9	36	7‐9	7‐9	NOUN
eurjchem-365	9	37	]	]	X
eurjchem-365	9	38	,	,	PUNCT
eurjchem-365	9	39	oxadiazoles	oxadiazole	NOUN
eurjchem-365	9	40	[	[	X
eurjchem-365	9	41	10	10	NUM
eurjchem-365	9	42	]	]	PUNCT
eurjchem-365	9	43	have	have	AUX
eurjchem-365	9	44	stimulated	stimulate	VERB
eurjchem-365	9	45	the	the	DET
eurjchem-365	9	46	authors	author	NOUN
eurjchem-365	9	47	to	to	PART
eurjchem-365	9	48	synthesize	synthesize	VERB
eurjchem-365	9	49	new	new	ADJ
eurjchem-365	9	50	derivatives	derivative	NOUN
eurjchem-365	9	51	of	of	ADP
eurjchem-365	9	52	these	these	DET
eurjchem-365	9	53	classes	class	NOUN
eurjchem-365	9	54	of	of	ADP
eurjchem-365	9	55	compounds	compound	NOUN
eurjchem-365	9	56	hoping	hope	VERB
eurjchem-365	9	57	to	to	PART
eurjchem-365	9	58	obtain	obtain	VERB
eurjchem-365	9	59	structures	structure	NOUN
eurjchem-365	9	60	with	with	ADP
eurjchem-365	9	61	possibly	possibly	ADV
eurjchem-365	9	62	enhanced	enhance	VERB
eurjchem-365	9	63	potency	potency	NOUN
eurjchem-365	9	64	.	.	PUNCT
eurjchem-365	10	1	in	in	ADP
eurjchem-365	10	2	continuation	continuation	NOUN
eurjchem-365	10	3	of	of	ADP
eurjchem-365	10	4	our	our	PRON
eurjchem-365	10	5	ongoing	ongoing	ADJ
eurjchem-365	10	6	program	program	NOUN
eurjchem-365	10	7	in	in	ADP
eurjchem-365	10	8	the	the	DET
eurjchem-365	10	9	synthesis	synthesis	NOUN
eurjchem-365	10	10	of	of	ADP
eurjchem-365	10	11	biologically	biologically	ADV
eurjchem-365	10	12	active	active	ADJ
eurjchem-365	10	13	heterocyclic	heterocyclic	ADJ
eurjchem-365	10	14	systems	system	NOUN
eurjchem-365	10	15	from	from	ADP
eurjchem-365	10	16	simple	simple	ADJ
eurjchem-365	10	17	readily	readily	ADV
eurjchem-365	10	18	obtainable	obtainable	ADJ
eurjchem-365	10	19	materials	material	NOUN
eurjchem-365	10	20	[	[	X
eurjchem-365	10	21	11‐21	11‐21	NUM
eurjchem-365	10	22	]	]	PUNCT
eurjchem-365	10	23	,	,	PUNCT
eurjchem-365	10	24	the	the	DET
eurjchem-365	10	25	present	present	ADJ
eurjchem-365	10	26	work	work	NOUN
eurjchem-365	10	27	investigates	investigate	VERB
eurjchem-365	10	28	the	the	DET
eurjchem-365	10	29	reactivity	reactivity	NOUN
eurjchem-365	10	30	of	of	ADP
eurjchem-365	10	31	high	high	ADJ
eurjchem-365	10	32	functionality	functionality	NOUN
eurjchem-365	10	33	2‐cyano‐3‐phenyl‐2‐propenoyl	2‐cyano‐3‐phenyl‐2‐propenoyl	PROPN
eurjchem-365	10	34	chloride	chloride	NOUN
eurjchem-365	11	1	[	[	X
eurjchem-365	11	2	22	22	NUM
eurjchem-365	11	3	]	]	PUNCT
eurjchem-365	11	4	(	(	PUNCT
eurjchem-365	11	5	1	1	X
eurjchem-365	11	6	)	)	PUNCT
eurjchem-365	11	7	with	with	ADP
eurjchem-365	11	8	different	different	ADJ
eurjchem-365	11	9	mono‐	mono‐	NOUN
eurjchem-365	11	10	and	and	CCONJ
eurjchem-365	11	11	bi‐dentate	bi‐dentate	ADJ
eurjchem-365	11	12	nucleophiles	nucleophile	NOUN
eurjchem-365	11	13	aiming	aim	VERB
eurjchem-365	11	14	to	to	PART
eurjchem-365	11	15	obtain	obtain	VERB
eurjchem-365	11	16	new	new	ADJ
eurjchem-365	11	17	derivatives	derivative	NOUN
eurjchem-365	11	18	with	with	ADP
eurjchem-365	11	19	anticipated	anticipated	ADJ
eurjchem-365	11	20	biological	biological	ADJ
eurjchem-365	11	21	activities	activity	NOUN
eurjchem-365	11	22	.	.	PUNCT
eurjchem-365	12	1	2	2	X
eurjchem-365	12	2	.	.	X
eurjchem-365	12	3	experimental	experimental	ADJ
eurjchem-365	12	4	melting	melting	NOUN
eurjchem-365	12	5	points	point	NOUN
eurjchem-365	12	6	reported	report	VERB
eurjchem-365	12	7	have	have	AUX
eurjchem-365	12	8	been	be	AUX
eurjchem-365	12	9	measured	measure	VERB
eurjchem-365	12	10	on	on	ADP
eurjchem-365	12	11	a	a	DET
eurjchem-365	12	12	stuart	stuart	PROPN
eurjchem-365	12	13	scientific	scientific	ADJ
eurjchem-365	12	14	melting	melting	NOUN
eurjchem-365	12	15	point	point	NOUN
eurjchem-365	12	16	apparatus	apparatus	NOUN
eurjchem-365	12	17	and	and	CCONJ
eurjchem-365	12	18	are	be	AUX
eurjchem-365	12	19	uncorrected	uncorrecte	VERB
eurjchem-365	12	20	.	.	PUNCT
eurjchem-365	13	1	the	the	DET
eurjchem-365	13	2	ir	ir	PROPN
eurjchem-365	13	3	spectra	spectra	PROPN
eurjchem-365	13	4	were	be	AUX
eurjchem-365	13	5	recorded	record	VERB
eurjchem-365	13	6	on	on	ADP
eurjchem-365	13	7	pye	pye	PROPN
eurjchem-365	13	8	unicam	unicam	ADV
eurjchem-365	13	9	sp	sp	ADP
eurjchem-365	13	10	1200	1200	NUM
eurjchem-365	13	11	spectrophotometer	spectrophotometer	NOUN
eurjchem-365	13	12	using	use	VERB
eurjchem-365	13	13	kbr	kbr	PROPN
eurjchem-365	13	14	wafer	wafer	NOUN
eurjchem-365	13	15	technique	technique	NOUN
eurjchem-365	13	16	.	.	PUNCT
eurjchem-365	14	1	1h	1h	NUM
eurjchem-365	14	2	nmr	nmr	PROPN
eurjchem-365	14	3	spectra	spectra	NOUN
eurjchem-365	14	4	were	be	AUX
eurjchem-365	14	5	determined	determine	VERB
eurjchem-365	14	6	on	on	ADP
eurjchem-365	14	7	a	a	DET
eurjchem-365	14	8	varian	varian	PROPN
eurjchem-365	14	9	ft‐200	ft‐200	PROPN
eurjchem-365	14	10	,	,	PUNCT
eurjchem-365	14	11	and	and	CCONJ
eurjchem-365	14	12	a	a	DET
eurjchem-365	14	13	bruker	bruker	NOUN
eurjchem-365	14	14	ac‐200	ac‐200	NOUN
eurjchem-365	14	15	mhz	mhz	ADJ
eurjchem-365	14	16	spectrometer	spectrometer	NOUN
eurjchem-365	14	17	using	use	VERB
eurjchem-365	14	18	tms	tms	PROPN
eurjchem-365	14	19	as	as	ADP
eurjchem-365	14	20	internal	internal	ADJ
eurjchem-365	14	21	standard	standard	NOUN
eurjchem-365	14	22	.	.	PUNCT
eurjchem-365	15	1	all	all	DET
eurjchem-365	15	2	chemical	chemical	ADJ
eurjchem-365	15	3	shifts	shift	NOUN
eurjchem-365	15	4	(	(	PUNCT
eurjchem-365	15	5	δ	δ	NOUN
eurjchem-365	15	6	)	)	PUNCT
eurjchem-365	15	7	are	be	AUX
eurjchem-365	15	8	expressed	express	VERB
eurjchem-365	15	9	in	in	ADP
eurjchem-365	15	10	ppm	ppm	NOUN
eurjchem-365	15	11	.	.	PUNCT
eurjchem-365	16	1	all	all	DET
eurjchem-365	16	2	the	the	DET
eurjchem-365	16	3	nh	nh	PROPN
eurjchem-365	16	4	or	or	CCONJ
eurjchem-365	16	5	oh	oh	NUM
eurjchem-365	16	6	protons	proton	NOUN
eurjchem-365	16	7	disappeared	disappear	VERB
eurjchem-365	16	8	on	on	ADP
eurjchem-365	16	9	addition	addition	NOUN
eurjchem-365	16	10	of	of	ADP
eurjchem-365	16	11	d2o	d2o	NOUN
eurjchem-365	16	12	.	.	PUNCT
eurjchem-365	17	1	the	the	DET
eurjchem-365	17	2	mass	mass	ADJ
eurjchem-365	17	3	spectra	spectra	NOUN
eurjchem-365	17	4	were	be	AUX
eurjchem-365	17	5	determined	determine	VERB
eurjchem-365	17	6	using	use	VERB
eurjchem-365	17	7	mp	mp	PROPN
eurjchem-365	17	8	model	model	NOUN
eurjchem-365	17	9	ms‐5988	ms‐5988	ADJ
eurjchem-365	17	10	and	and	CCONJ
eurjchem-365	17	11	shimadzu	shimadzu	ADJ
eurjchem-365	17	12	single	single	ADJ
eurjchem-365	17	13	focusing	focus	VERB
eurjchem-365	17	14	mass	mass	NOUN
eurjchem-365	17	15	spectrophotometer	spectrophotometer	NOUN
eurjchem-365	17	16	(	(	PUNCT
eurjchem-365	17	17	70	70	NUM
eurjchem-365	17	18	ev	ev	NOUN
eurjchem-365	17	19	)	)	PUNCT
eurjchem-365	17	20	.	.	PUNCT
eurjchem-365	18	1	compound	compound	NOUN
eurjchem-365	18	2	1	1	NUM
eurjchem-365	18	3	has	have	AUX
eurjchem-365	18	4	been	be	AUX
eurjchem-365	18	5	synthesized	synthesize	VERB
eurjchem-365	18	6	according	accord	VERB
eurjchem-365	18	7	to	to	ADP
eurjchem-365	18	8	jaafar	jaafar	PROPN
eurjchem-365	18	9	et	et	PROPN
eurjchem-365	18	10	al	al	PROPN
eurjchem-365	18	11	.	.	PROPN
eurjchem-365	18	12	method	method	PROPN
eurjchem-365	19	1	[	[	X
eurjchem-365	19	2	22	22	NUM
eurjchem-365	19	3	]	]	PUNCT
eurjchem-365	19	4	.	.	PUNCT
eurjchem-365	20	1	the	the	DET
eurjchem-365	20	2	conduction	conduction	NOUN
eurjchem-365	20	3	time	time	NOUN
eurjchem-365	20	4	of	of	ADP
eurjchem-365	20	5	all	all	DET
eurjchem-365	20	6	reactions	reaction	NOUN
eurjchem-365	20	7	and	and	CCONJ
eurjchem-365	20	8	the	the	DET
eurjchem-365	20	9	purity	purity	NOUN
eurjchem-365	20	10	of	of	ADP
eurjchem-365	20	11	the	the	DET
eurjchem-365	20	12	products	product	NOUN
eurjchem-365	20	13	were	be	AUX
eurjchem-365	20	14	monitored	monitor	VERB
eurjchem-365	20	15	using	use	VERB
eurjchem-365	20	16	thin‐layer	thin‐layer	NOUN
eurjchem-365	20	17	chromatography	chromatography	NOUN
eurjchem-365	20	18	(	(	PUNCT
eurjchem-365	20	19	tlc	tlc	NOUN
eurjchem-365	20	20	)	)	PUNCT
eurjchem-365	20	21	technique	technique	NOUN
eurjchem-365	20	22	.	.	PUNCT
eurjchem-365	21	1	2.1	2.1	NUM
eurjchem-365	21	2	.	.	PUNCT
eurjchem-365	21	3	n‐[2‐cyano‐3‐phenyl‐2‐propenoyl]benzylamine	n‐[2‐cyano‐3‐phenyl‐2‐propenoyl]benzylamine	PROPN
eurjchem-365	21	4	(	(	PUNCT
eurjchem-365	21	5	2	2	NUM
eurjchem-365	21	6	)	)	PUNCT
eurjchem-365	21	7	to	to	ADP
eurjchem-365	21	8	a	a	DET
eurjchem-365	21	9	solution	solution	NOUN
eurjchem-365	21	10	of	of	ADP
eurjchem-365	21	11	propenoyl	propenoyl	PROPN
eurjchem-365	21	12	chloride	chloride	NOUN
eurjchem-365	21	13	(	(	PUNCT
eurjchem-365	21	14	1	1	NUM
eurjchem-365	21	15	)	)	PUNCT
eurjchem-365	21	16	(	(	PUNCT
eurjchem-365	21	17	1.9	1.9	NUM
eurjchem-365	21	18	g	g	NOUN
eurjchem-365	21	19	;	;	PUNCT
eurjchem-365	21	20	10	10	NUM
eurjchem-365	21	21	mmol	mmol	NOUN
eurjchem-365	21	22	)	)	PUNCT
eurjchem-365	21	23	in	in	ADP
eurjchem-365	21	24	dry	dry	ADJ
eurjchem-365	21	25	benzene	benzene	NOUN
eurjchem-365	21	26	(	(	PUNCT
eurjchem-365	21	27	30	30	NUM
eurjchem-365	21	28	ml	ml	NOUN
eurjchem-365	21	29	)	)	PUNCT
eurjchem-365	21	30	in	in	ADP
eurjchem-365	21	31	presence	presence	NOUN
eurjchem-365	21	32	of	of	ADP
eurjchem-365	21	33	triethylamine	triethylamine	NOUN
eurjchem-365	21	34	(	(	PUNCT
eurjchem-365	21	35	1.38	1.38	NUM
eurjchem-365	21	36	ml	ml	NOUN
eurjchem-365	21	37	;	;	PUNCT
eurjchem-365	21	38	10	10	NUM
eurjchem-365	21	39	mmol	mmol	NOUN
eurjchem-365	21	40	)	)	PUNCT
eurjchem-365	21	41	,	,	PUNCT
eurjchem-365	21	42	benzylamine	benzylamine	NOUN
eurjchem-365	21	43	(	(	PUNCT
eurjchem-365	21	44	1.08	1.08	NUM
eurjchem-365	21	45	ml	ml	NOUN
eurjchem-365	21	46	;	;	PUNCT
eurjchem-365	21	47	10	10	NUM
eurjchem-365	21	48	mmol	mmol	NOUN
eurjchem-365	21	49	)	)	PUNCT
eurjchem-365	21	50	was	be	AUX
eurjchem-365	21	51	added	add	VERB
eurjchem-365	21	52	and	and	CCONJ
eurjchem-365	21	53	the	the	DET
eurjchem-365	21	54	reaction	reaction	NOUN
eurjchem-365	21	55	mixture	mixture	NOUN
eurjchem-365	21	56	was	be	AUX
eurjchem-365	21	57	stirred	stir	VERB
eurjchem-365	21	58	at	at	ADP
eurjchem-365	21	59	room	room	NOUN
eurjchem-365	21	60	temperature	temperature	NOUN
eurjchem-365	21	61	for	for	ADP
eurjchem-365	21	62	an	an	DET
eurjchem-365	21	63	hour	hour	NOUN
eurjchem-365	21	64	.	.	PUNCT
eurjchem-365	22	1	the	the	DET
eurjchem-365	22	2	solid	solid	ADJ
eurjchem-365	22	3	formed	form	VERB
eurjchem-365	22	4	was	be	AUX
eurjchem-365	22	5	collected	collect	VERB
eurjchem-365	22	6	,	,	PUNCT
eurjchem-365	22	7	washed	wash	VERB
eurjchem-365	22	8	with	with	ADP
eurjchem-365	22	9	water	water	NOUN
eurjchem-365	22	10	several	several	ADJ
eurjchem-365	22	11	times	time	NOUN
eurjchem-365	22	12	,	,	PUNCT
eurjchem-365	22	13	dried	dry	VERB
eurjchem-365	22	14	and	and	CCONJ
eurjchem-365	22	15	crystallized	crystallize	VERB
eurjchem-365	22	16	from	from	ADP
eurjchem-365	22	17	benzene	benzene	NOUN
eurjchem-365	22	18	to	to	PART
eurjchem-365	22	19	yield	yield	VERB
eurjchem-365	22	20	2	2	NUM
eurjchem-365	22	21	as	as	ADP
eurjchem-365	22	22	colourless	colourless	ADJ
eurjchem-365	22	23	crystals	crystal	NOUN
eurjchem-365	22	24	(	(	PUNCT
eurjchem-365	22	25	scheme	scheme	NOUN
eurjchem-365	22	26	1	1	NUM
eurjchem-365	22	27	)	)	PUNCT
eurjchem-365	22	28	.	.	PUNCT
eurjchem-365	23	1	yield	yield	NOUN
eurjchem-365	23	2	:	:	PUNCT
eurjchem-365	23	3	60	60	NUM
eurjchem-365	23	4	%	%	NOUN
eurjchem-365	23	5	.	.	PUNCT
eurjchem-365	24	1	m.p	m.p	PROPN
eurjchem-365	24	2	.	.	PROPN
eurjchem-365	24	3	:	:	PUNCT
eurjchem-365	25	1	135‐137	135‐137	NUM
eurjchem-365	25	2	oc	oc	NOUN
eurjchem-365	25	3	.	.	PUNCT
eurjchem-365	25	4	ft‐ir	ft‐ir	NOUN
eurjchem-365	25	5	(	(	PUNCT
eurjchem-365	25	6	kbr	kbr	PROPN
eurjchem-365	25	7	,	,	PUNCT
eurjchem-365	25	8	cm‐1	cm‐1	PROPN
eurjchem-365	25	9	):	):	PUNCT
eurjchem-365	25	10	3337	3337	NUM
eurjchem-365	25	11	(nh	(nh	NOUN
eurjchem-365	25	12	)	)	PUNCT
eurjchem-365	25	13	,	,	PUNCT
eurjchem-365	25	14	2220	2220	NUM
eurjchem-365	25	15	(cn	(cn	NOUN
eurjchem-365	25	16	)	)	PUNCT
eurjchem-365	25	17	,	,	PUNCT
eurjchem-365	25	18	1663	1663	NUM
eurjchem-365	25	19	(c	(c	NOUN
eurjchem-365	25	20	=	=	SYM
eurjchem-365	25	21	o	o	NOUN
eurjchem-365	25	22	)	)	PUNCT
eurjchem-365	25	23	(	(	PUNCT
eurjchem-365	25	24	amide	amide	NOUN
eurjchem-365	25	25	)	)	PUNCT
eurjchem-365	25	26	.	.	PUNCT
eurjchem-365	26	1	1h	1h	NUM
eurjchem-365	26	2	nmr	nmr	NOUN
eurjchem-365	26	3	(	(	PUNCT
eurjchem-365	26	4	300	300	NUM
eurjchem-365	26	5	mhz	mhz	NOUN
eurjchem-365	26	6	,	,	PUNCT
eurjchem-365	26	7	dmso‐d6	dmso‐d6	NUM
eurjchem-365	26	8	):	):	PUNCT
eurjchem-365	26	9	4.44	4.44	NUM
eurjchem-365	26	10	(	(	PUNCT
eurjchem-365	26	11	d	d	PROPN
eurjchem-365	26	12	,	,	PUNCT
eurjchem-365	26	13	2h	2h	NUM
eurjchem-365	26	14	,	,	PUNCT
eurjchem-365	26	15	j	j	PROPN
eurjchem-365	26	16	=	=	SYM
eurjchem-365	26	17	20	20	NUM
eurjchem-365	26	18	hz	hz	NOUN
eurjchem-365	26	19	,	,	PUNCT
eurjchem-365	26	20	ch2‐nh	ch2‐nh	NOUN
eurjchem-365	26	21	)	)	PUNCT
eurjchem-365	26	22	,	,	PUNCT
eurjchem-365	26	23	7.24‐7.95	7.24‐7.95	NUM
eurjchem-365	26	24	(	(	PUNCT
eurjchem-365	26	25	m	m	PROPN
eurjchem-365	26	26	,	,	PUNCT
eurjchem-365	26	27	10h	10h	NUM
eurjchem-365	26	28	,	,	PUNCT
eurjchem-365	26	29	ar‐h	ar‐h	PROPN
eurjchem-365	26	30	)	)	PUNCT
eurjchem-365	26	31	,	,	PUNCT
eurjchem-365	26	32	8.21	8.21	NUM
eurjchem-365	26	33	(	(	PUNCT
eurjchem-365	26	34	s	s	PROPN
eurjchem-365	26	35	,	,	PUNCT
eurjchem-365	26	36	1h	1h	NUM
eurjchem-365	26	37	,	,	PUNCT
eurjchem-365	26	38	=	=	NOUN
eurjchem-365	26	39	ch	ch	NOUN
eurjchem-365	26	40	)	)	PUNCT
eurjchem-365	26	41	,	,	PUNCT
eurjchem-365	26	42	8.97	8.97	NUM
eurjchem-365	26	43	(	(	PUNCT
eurjchem-365	26	44	t	t	PROPN
eurjchem-365	26	45	,	,	PUNCT
eurjchem-365	26	46	1h	1h	NUM
eurjchem-365	26	47	,	,	PUNCT
eurjchem-365	26	48	j	j	PROPN
eurjchem-365	26	49	=	=	SYM
eurjchem-365	26	50	20	20	NUM
eurjchem-365	26	51	hz	hz	VERB
eurjchem-365	26	52	,	,	PUNCT
eurjchem-365	26	53	nh‐ch2	nh‐ch2	ADJ
eurjchem-365	26	54	)	)	PUNCT
eurjchem-365	26	55	.	.	PUNCT
eurjchem-365	27	1	ms	ms	NOUN
eurjchem-365	27	2	(	(	PUNCT
eurjchem-365	27	3	ei	ei	PROPN
eurjchem-365	27	4	,	,	PUNCT
eurjchem-365	27	5	m	m	PROPN
eurjchem-365	27	6	/	/	SYM
eurjchem-365	27	7	z	z	X
eurjchem-365	27	8	):	):	PUNCT
eurjchem-365	27	9	262	262	NUM
eurjchem-365	27	10	(	(	PUNCT
eurjchem-365	27	11	m.+	m.+	NOUN
eurjchem-365	27	12	)	)	PUNCT
eurjchem-365	27	13	.	.	PUNCT
eurjchem-365	28	1	anal	anal	PROPN
eurjchem-365	28	2	.	.	PUNCT
eurjchem-365	28	3	calcd	calcd	NOUN
eurjchem-365	28	4	.	.	PUNCT
eurjchem-365	29	1	for	for	ADP
eurjchem-365	29	2	c17h14n2o	c17h14n2o	NOUN
eurjchem-365	29	3	:	:	PUNCT
eurjchem-365	29	4	c	c	X
eurjchem-365	29	5	,	,	PUNCT
eurjchem-365	29	6	77.86	77.86	NUM
eurjchem-365	29	7	;	;	PUNCT
eurjchem-365	29	8	h	h	NOUN
eurjchem-365	29	9	,	,	PUNCT
eurjchem-365	29	10	5.34	5.34	NUM
eurjchem-365	29	11	;	;	PUNCT
eurjchem-365	29	12	n	n	CCONJ
eurjchem-365	29	13	,	,	PUNCT
eurjchem-365	29	14	10.68	10.68	NUM
eurjchem-365	29	15	.	.	PUNCT
eurjchem-365	29	16	found	find	VERB
eurjchem-365	29	17	:	:	PUNCT
eurjchem-365	30	1	c	c	X
eurjchem-365	30	2	,	,	PUNCT
eurjchem-365	30	3	77.54	77.54	NUM
eurjchem-365	30	4	;	;	PUNCT
eurjchem-365	30	5	h	h	NOUN
eurjchem-365	30	6	,	,	PUNCT
eurjchem-365	30	7	5.66	5.66	NUM
eurjchem-365	30	8	;	;	PUNCT
eurjchem-365	30	9	n	n	CCONJ
eurjchem-365	30	10	,	,	PUNCT
eurjchem-365	30	11	10.29	10.29	NUM
eurjchem-365	30	12	%	%	NOUN
eurjchem-365	30	13	.	.	PUNCT
eurjchem-365	31	1	2.2	2.2	NUM
eurjchem-365	31	2	.	.	PUNCT
eurjchem-365	31	3	n‐(4‐methoxyphenyl)2‐cyano‐3‐phenyl‐2‐propenoyl	n‐(4‐methoxyphenyl)2‐cyano‐3‐phenyl‐2‐propenoyl	ADJ
eurjchem-365	31	4	amide	amide	NOUN
eurjchem-365	31	5	(	(	PUNCT
eurjchem-365	31	6	3	3	NUM
eurjchem-365	31	7	)	)	PUNCT
eurjchem-365	31	8	to	to	ADP
eurjchem-365	31	9	a	a	DET
eurjchem-365	31	10	solution	solution	NOUN
eurjchem-365	31	11	of	of	ADP
eurjchem-365	31	12	1	1	NUM
eurjchem-365	31	13	(	(	PUNCT
eurjchem-365	31	14	1.9	1.9	NUM
eurjchem-365	31	15	g	g	NOUN
eurjchem-365	31	16	;	;	PUNCT
eurjchem-365	31	17	10	10	NUM
eurjchem-365	31	18	mmol	mmol	NOUN
eurjchem-365	31	19	)	)	PUNCT
eurjchem-365	31	20	in	in	ADP
eurjchem-365	31	21	dry	dry	ADJ
eurjchem-365	31	22	benzene	benzene	NOUN
eurjchem-365	31	23	(	(	PUNCT
eurjchem-365	31	24	30	30	NUM
eurjchem-365	31	25	ml	ml	NOUN
eurjchem-365	31	26	)	)	PUNCT
eurjchem-365	31	27	in	in	ADP
eurjchem-365	31	28	presence	presence	NOUN
eurjchem-365	31	29	of	of	ADP
eurjchem-365	31	30	triethylamine	triethylamine	NOUN
eurjchem-365	31	31	(	(	PUNCT
eurjchem-365	31	32	1.38	1.38	NUM
eurjchem-365	31	33	ml	ml	NOUN
eurjchem-365	31	34	;	;	PUNCT
eurjchem-365	31	35	10	10	NUM
eurjchem-365	31	36	mmol	mmol	NOUN
eurjchem-365	31	37	)	)	PUNCT
eurjchem-365	31	38	,	,	PUNCT
eurjchem-365	31	39	p‐anisidine	p‐anisidine	PUNCT
eurjchem-365	31	40	(	(	PUNCT
eurjchem-365	31	41	1.22	1.22	NUM
eurjchem-365	31	42	g	g	NOUN
eurjchem-365	31	43	;	;	PUNCT
eurjchem-365	31	44	10	10	NUM
eurjchem-365	31	45	mmol	mmol	NOUN
eurjchem-365	31	46	)	)	PUNCT
eurjchem-365	31	47	was	be	AUX
eurjchem-365	31	48	added	add	VERB
eurjchem-365	31	49	.	.	PUNCT
eurjchem-365	32	1	the	the	DET
eurjchem-365	32	2	reaction	reaction	NOUN
eurjchem-365	32	3	mixture	mixture	NOUN
eurjchem-365	32	4	was	be	AUX
eurjchem-365	32	5	stirred	stir	VERB
eurjchem-365	32	6	at	at	ADP
eurjchem-365	32	7	room	room	NOUN
eurjchem-365	32	8	temperature	temperature	NOUN
eurjchem-365	32	9	for	for	ADP
eurjchem-365	32	10	an	an	DET
eurjchem-365	32	11	hour	hour	NOUN
eurjchem-365	32	12	.	.	PUNCT
eurjchem-365	33	1	the	the	DET
eurjchem-365	33	2	semisolid	semisolid	NOUN
eurjchem-365	33	3	produced	produce	VERB
eurjchem-365	33	4	was	be	AUX
eurjchem-365	33	5	collected	collect	VERB
eurjchem-365	33	6	,	,	PUNCT
eurjchem-365	33	7	washed	wash	VERB
eurjchem-365	33	8	with	with	ADP
eurjchem-365	33	9	water	water	NOUN
eurjchem-365	33	10	several	several	ADJ
eurjchem-365	33	11	times	time	NOUN
eurjchem-365	33	12	,	,	PUNCT
eurjchem-365	33	13	and	and	CCONJ
eurjchem-365	33	14	then	then	ADV
eurjchem-365	33	15	triturated	triturate	VERB
eurjchem-365	33	16	with	with	ADP
eurjchem-365	33	17	methyl	methyl	NOUN
eurjchem-365	33	18	alcohol	alcohol	NOUN
eurjchem-365	33	19	.	.	PUNCT
eurjchem-365	34	1	the	the	DET
eurjchem-365	34	2	solid	solid	ADJ
eurjchem-365	34	3	separated	separate	VERB
eurjchem-365	34	4	was	be	AUX
eurjchem-365	34	5	collected	collect	VERB
eurjchem-365	34	6	,	,	PUNCT
eurjchem-365	34	7	dried	dry	VERB
eurjchem-365	34	8	and	and	CCONJ
eurjchem-365	34	9	crystallized	crystallize	VERB
eurjchem-365	34	10	from	from	ADP
eurjchem-365	34	11	methanol	methanol	NOUN
eurjchem-365	34	12	to	to	PART
eurjchem-365	34	13	give	give	VERB
eurjchem-365	34	14	3	3	NUM
eurjchem-365	34	15	as	as	ADP
eurjchem-365	34	16	yellow	yellow	ADJ
eurjchem-365	34	17	crystals	crystal	NOUN
eurjchem-365	34	18	(	(	PUNCT
eurjchem-365	34	19	scheme	scheme	NOUN
eurjchem-365	34	20	1	1	NUM
eurjchem-365	34	21	)	)	PUNCT
eurjchem-365	34	22	.	.	PUNCT
eurjchem-365	35	1	yield	yield	NOUN
eurjchem-365	35	2	:	:	PUNCT
eurjchem-365	35	3	60	60	NUM
eurjchem-365	35	4	%	%	NOUN
eurjchem-365	35	5	.	.	PUNCT
eurjchem-365	36	1	m.p	m.p	PROPN
eurjchem-365	36	2	.	.	PROPN
eurjchem-365	36	3	:	:	PUNCT
eurjchem-365	37	1	155‐157	155‐157	NUM
eurjchem-365	37	2	oc	oc	NOUN
eurjchem-365	37	3	.	.	PUNCT
eurjchem-365	37	4	ft‐ir	ft‐ir	NOUN
eurjchem-365	37	5	(	(	PUNCT
eurjchem-365	37	6	kbr	kbr	PROPN
eurjchem-365	37	7	,	,	PUNCT
eurjchem-365	37	8	cm‐1	cm‐1	PROPN
eurjchem-365	37	9	):	):	PUNCT
eurjchem-365	37	10	3312	3312	NUM
eurjchem-365	37	11	(nh	(nh	PROPN
eurjchem-365	37	12	)	)	PUNCT
eurjchem-365	37	13	,	,	PUNCT
eurjchem-365	37	14	2220	2220	NUM
eurjchem-365	37	15	(cn	(cn	NOUN
eurjchem-365	37	16	)	)	PUNCT
eurjchem-365	37	17	,	,	PUNCT
eurjchem-365	37	18	1676	1676	NUM
eurjchem-365	37	19	(c	(c	PROPN
eurjchem-365	37	20	=	=	SYM
eurjchem-365	37	21	o	o	NOUN
eurjchem-365	37	22	)	)	PUNCT
eurjchem-365	37	23	(	(	PUNCT
eurjchem-365	37	24	amide	amide	NOUN
eurjchem-365	37	25	)	)	PUNCT
eurjchem-365	37	26	.	.	PUNCT
eurjchem-365	38	1	shiba	shiba	PROPN
eurjchem-365	38	2	et	et	PROPN
eurjchem-365	38	3	al	al	PROPN
eurjchem-365	38	4	.	.	PUNCT
eurjchem-365	38	5	/	/	SYM
eurjchem-365	38	6	european	european	PROPN
eurjchem-365	38	7	journal	journal	PROPN
eurjchem-365	38	8	of	of	ADP
eurjchem-365	38	9	chemistry	chemistry	NOUN
eurjchem-365	38	10	2	2	NUM
eurjchem-365	38	11	(	(	PUNCT
eurjchem-365	38	12	2	2	NUM
eurjchem-365	38	13	)	)	PUNCT
eurjchem-365	38	14	(	(	PUNCT
eurjchem-365	38	15	2011	2011	NUM
eurjchem-365	38	16	)	)	PUNCT
eurjchem-365	38	17	200‐205	200‐205	NUM
eurjchem-365	38	18	201	201	NUM
eurjchem-365	38	19	ar	ar	NOUN
eurjchem-365	38	20	c	c	NOUN
eurjchem-365	38	21	o	o	PROPN
eurjchem-365	38	22	cl	cl	PROPN
eurjchem-365	38	23	ar	ar	PROPN
eurjchem-365	38	24	c	c	NOUN
eurjchem-365	38	25	o	o	NOUN
eurjchem-365	38	26	x	x	X
eurjchem-365	38	27	ar	ar	ADP
eurjchem-365	38	28	`	`	PUNCT
eurjchem-365	38	29	r	r	NOUN
eurjchem-365	38	30	-	-	PUNCT
eurjchem-365	38	31	nh2	nh2	NOUN
eurjchem-365	38	32	nh2	nh2	PROPN
eurjchem-365	38	33	nh2	nh2	PROPN
eurjchem-365	38	34	nh2oh	nh2oh	PROPN
eurjchem-365	38	35	nh	nh	PROPN
eurjchem-365	38	36	-	-	PUNCT
eurjchem-365	38	37	co	co	NOUN
eurjchem-365	38	38	-	-	PROPN
eurjchem-365	38	39	ar	ar	NOUN
eurjchem-365	38	40	nh	nh	PROPN
eurjchem-365	38	41	-	-	PUNCT
eurjchem-365	38	42	co	co	NOUN
eurjchem-365	38	43	-	-	NOUN
eurjchem-365	38	44	ar	ar	NOUN
eurjchem-365	38	45	ar	ar	PROPN
eurjchem-365	38	46	c	c	PROPN
eurjchem-365	38	47	o	o	PROPN
eurjchem-365	38	48	h	h	NOUN
eurjchem-365	38	49	n	n	CCONJ
eurjchem-365	38	50	r	r	NOUN
eurjchem-365	38	51	ar	ar	NOUN
eurjchem-365	39	1	c	c	NOUN
eurjchem-365	39	2	o	o	NOUN
eurjchem-365	39	3	o	o	X
eurjchem-365	39	4	ch2	ch2	PROPN
eurjchem-365	39	5	ch2	ch2	PROPN
eurjchem-365	39	6	hn	hn	PROPN
eurjchem-365	39	7	c	c	PROPN
eurjchem-365	39	8	o	o	PROPN
eurjchem-365	39	9	ar	ar	PROPN
eurjchem-365	39	10	cn	cn	PROPN
eurjchem-365	39	11	h	h	PROPN
eurjchem-365	39	12	ar`-xh	ar`-xh	NOUN
eurjchem-365	39	13	n	n	PROPN
eurjchem-365	39	14	h	h	PROPN
eurjchem-365	39	15	n	n	X
eurjchem-365	39	16	ar	ar	PROPN
eurjchem-365	39	17	alcl3	alcl3	PROPN
eurjchem-365	40	1	n	n	NUM
eurjchem-365	40	2	h	h	NOUN
eurjchem-365	41	1	cn	cn	NOUN
eurjchem-365	41	2	o	o	X
eurjchem-365	41	3	(	(	PUNCT
eurjchem-365	41	4	1	1	NUM
eurjchem-365	41	5	)	)	PUNCT
eurjchem-365	41	6	(	(	PUNCT
eurjchem-365	41	7	8)	8)	NUM
eurjchem-365	41	8	(	(	PUNCT
eurjchem-365	41	9	7	7	NUM
eurjchem-365	41	10	)	)	PUNCT
eurjchem-365	41	11	2	2	NUM
eurjchem-365	41	12	)	)	PUNCT
eurjchem-365	41	13	r	r	NOUN
eurjchem-365	41	14	=	=	PUNCT
eurjchem-365	41	15	c6h5	c6h5	NOUN
eurjchem-365	41	16	-	-	ADJ
eurjchem-365	41	17	ch23	ch23	PROPN
eurjchem-365	41	18	)	)	PUNCT
eurjchem-365	41	19	=	=	PUNCT
eurjchem-365	42	1	c6h4	c6h4	NOUN
eurjchem-365	42	2	-	-	PUNCT
eurjchem-365	42	3	och3	och3	ADJ
eurjchem-365	42	4	(	(	PUNCT
eurjchem-365	42	5	4	4	NUM
eurjchem-365	42	6	)	)	PUNCT
eurjchem-365	42	7	5	5	NUM
eurjchem-365	42	8	)	)	PUNCT
eurjchem-365	42	9	x	x	X
eurjchem-365	43	1	=	=	SYM
eurjchem-365	43	2	o	o	NOUN
eurjchem-365	43	3	,	,	PUNCT
eurjchem-365	43	4	ar	ar	NOUN
eurjchem-365	43	5	`	`	PUNCT
eurjchem-365	43	6	=	=	PUNCT
eurjchem-365	43	7	c6h4	c6h4	X
eurjchem-365	43	8	-	-	PUNCT
eurjchem-365	43	9	ch3(2	ch3(2	NOUN
eurjchem-365	43	10	)	)	PUNCT
eurjchem-365	43	11	6	6	NUM
eurjchem-365	43	12	)	)	PUNCT
eurjchem-365	43	13	=	=	SYM
eurjchem-365	44	1	s	s	X
eurjchem-365	44	2	,	,	PUNCT
eurjchem-365	44	3	=	=	PUNCT
eurjchem-365	44	4	c6h4	c6h4	NOUN
eurjchem-365	44	5	-	-	NOUN
eurjchem-365	44	6	ch3(4	ch3(4	NOUN
eurjchem-365	44	7	)	)	PUNCT
eurjchem-365	44	8	ar	ar	NOUN
eurjchem-365	44	9	=	=	PROPN
eurjchem-365	44	10	pocl3	pocl3	PROPN
eurjchem-365	44	11	or	or	CCONJ
eurjchem-365	44	12	d	d	NOUN
eurjchem-365	44	13	(	(	PUNCT
eurjchem-365	44	14	b	b	NOUN
eurjchem-365	44	15	)	)	PUNCT
eurjchem-365	44	16	(	(	PUNCT
eurjchem-365	44	17	a	a	X
eurjchem-365	44	18	)	)	PUNCT
eurjchem-365	44	19	h3co	h3co	PUNCT
eurjchem-365	44	20	nh2	nh2	PROPN
eurjchem-365	44	21	cooh	cooh	VERB
eurjchem-365	44	22	et3n	et3n	PROPN
eurjchem-365	44	23	/	/	SYM
eurjchem-365	44	24	bz	bz	PROPN
eurjchem-365	44	25	or	or	CCONJ
eurjchem-365	44	26	pyr./r.t	pyr./r.t	VERB
eurjchem-365	44	27	pyri	pyri	NOUN
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eurjchem-365	44	29	ref	ref	NOUN
eurjchem-365	44	30	.	.	PUNCT
eurjchem-365	45	1	ar	ar	PROPN
eurjchem-365	45	2	c	c	NOUN
eurjchem-365	46	1	o	o	PROPN
eurjchem-365	46	2	h	h	NOUN
eurjchem-365	46	3	n	n	ADV
eurjchem-365	46	4	hooc	hooc	ADV
eurjchem-365	46	5	(	(	PUNCT
eurjchem-365	46	6	9	9	X
eurjchem-365	46	7	)	)	PUNCT
eurjchem-365	46	8	ac2o	ac2o	PROPN
eurjchem-365	46	9	n	n	NUM
eurjchem-365	46	10	o	o	NOUN
eurjchem-365	46	11	o	o	X
eurjchem-365	46	12	ar	ar	PROPN
eurjchem-365	46	13	n	n	PROPN
eurjchem-365	46	14	nh	nh	PROPN
eurjchem-365	46	15	o	o	PROPN
eurjchem-365	46	16	ar	ar	PROPN
eurjchem-365	46	17	aconh4	aconh4	PROPN
eurjchem-365	46	18	(	(	PUNCT
eurjchem-365	46	19	10	10	NUM
eurjchem-365	46	20	)	)	PUNCT
eurjchem-365	46	21	(	(	PUNCT
eurjchem-365	46	22	11	11	NUM
eurjchem-365	46	23	)	)	SYM
eurjchem-365	46	24	140	140	NUM
eurjchem-365	46	25	-	-	SYM
eurjchem-365	46	26	160	160	NUM
eurjchem-365	46	27	°	°	NOUN
eurjchem-365	46	28	c	c	NOUN
eurjchem-365	46	29	n2h4	n2h4	ADJ
eurjchem-365	46	30	/	/	SYM
eurjchem-365	46	31	etoh	etoh	NOUN
eurjchem-365	46	32	conh	conh	NOUN
eurjchem-365	46	33	-	-	PUNCT
eurjchem-365	46	34	n	n	CCONJ
eurjchem-365	46	35	=	=	NOUN
eurjchem-365	46	36	ch	ch	NOUN
eurjchem-365	46	37	-	-	PUNCT
eurjchem-365	46	38	ph	ph	ADJ
eurjchem-365	46	39	nh	nh	PROPN
eurjchem-365	46	40	-	-	PUNCT
eurjchem-365	46	41	co	co	NOUN
eurjchem-365	46	42	-	-	ADJ
eurjchem-365	46	43	ch2	ch2	NOUN
eurjchem-365	46	44	-	-	PUNCT
eurjchem-365	46	45	cn	cn	PROPN
eurjchem-365	46	46	(	(	PUNCT
eurjchem-365	46	47	15	15	NUM
eurjchem-365	46	48	)	)	PUNCT
eurjchem-365	46	49	n	n	CCONJ
eurjchem-365	46	50	n	n	ADV
eurjchem-365	46	51	o	o	NOUN
eurjchem-365	46	52	ar	ar	NOUN
eurjchem-365	46	53	hooc	hooc	ADV
eurjchem-365	46	54	ac2o	ac2o	PROPN
eurjchem-365	46	55	n	n	ADP
eurjchem-365	46	56	o	o	NOUN
eurjchem-365	46	57	o	o	NOUN
eurjchem-365	47	1	hn	hn	INTJ
eurjchem-365	47	2	c	c	PROPN
eurjchem-365	47	3	o	o	PROPN
eurjchem-365	47	4	ar	ar	PROPN
eurjchem-365	47	5	(	(	PUNCT
eurjchem-365	47	6	12	12	NUM
eurjchem-365	47	7	)	)	PUNCT
eurjchem-365	47	8	+	+	CCONJ
eurjchem-365	47	9	(	(	PUNCT
eurjchem-365	47	10	14	14	NUM
eurjchem-365	47	11	)	)	PUNCT
eurjchem-365	47	12	+	+	CCONJ
eurjchem-365	47	13	(	(	PUNCT
eurjchem-365	47	14	10	10	NUM
eurjchem-365	47	15	)	)	PUNCT
eurjchem-365	47	16	+	+	CCONJ
eurjchem-365	47	17	(	(	PUNCT
eurjchem-365	47	18	12	12	NUM
eurjchem-365	47	19	)	)	PUNCT
eurjchem-365	47	20	(	(	PUNCT
eurjchem-365	47	21	b	b	X
eurjchem-365	47	22	)	)	PUNCT
eurjchem-365	47	23	(	(	PUNCT
eurjchem-365	47	24	a	a	X
eurjchem-365	47	25	)	)	PUNCT
eurjchem-365	47	26	-h2o	-h2o	NOUN
eurjchem-365	47	27	-h2o	-h2o	NOUN
eurjchem-365	47	28	h	h	PROPN
eurjchem-365	47	29	ncar	ncar	NOUN
eurjchem-365	48	1	o	o	INTJ
eurjchem-365	48	2	co	co	VERB
eurjchem-365	48	3	hn	hn	PROPN
eurjchem-365	48	4	hooc	hooc	ADV
eurjchem-365	48	5	(	(	PUNCT
eurjchem-365	48	6	13	13	NUM
eurjchem-365	48	7	)	)	PUNCT
eurjchem-365	48	8	cooh	cooh	NOUN
eurjchem-365	48	9	nh2	nh2	PROPN
eurjchem-365	48	10	cooh	cooh	NOUN
eurjchem-365	48	11	nh2	nh2	PROPN
eurjchem-365	48	12	(	(	PUNCT
eurjchem-365	48	13	a	a	NOUN
eurjchem-365	48	14	)	)	PUNCT
eurjchem-365	48	15	etoh	etoh	NOUN
eurjchem-365	48	16	12:13	12:13	NUM
eurjchem-365	48	17	=	=	SYM
eurjchem-365	48	18	10:90	10:90	NUM
eurjchem-365	48	19	%	%	NOUN
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eurjchem-365	48	21	12:13	12:13	NUM
eurjchem-365	48	22	=	=	SYM
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eurjchem-365	48	24	%	%	NOUN
eurjchem-365	48	25	nh2	nh2	NOUN
eurjchem-365	48	26	cooh	cooh	NOUN
eurjchem-365	48	27	n	n	DET
eurjchem-365	48	28	nh2	nh2	PROPN
eurjchem-365	48	29	n	n	CCONJ
eurjchem-365	48	30	n	n	NOUN
eurjchem-365	48	31	o	o	NOUN
eurjchem-365	48	32	cnph	cnph	ADJ
eurjchem-365	48	33	phconhnh2	phconhnh2	NOUN
eurjchem-365	49	1	oh	oh	INTJ
eurjchem-365	50	1	nh2	nh2	PROPN
eurjchem-365	50	2	h	h	PROPN
eurjchem-365	50	3	nc	nc	PROPN
eurjchem-365	50	4	o	o	PROPN
eurjchem-365	50	5	ar	ar	PROPN
eurjchem-365	50	6	ho	ho	PROPN
eurjchem-365	50	7	c	c	PROPN
eurjchem-365	50	8	o	o	PROPN
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eurjchem-365	50	10	c	c	NOUN
eurjchem-365	50	11	o	o	PROPN
eurjchem-365	51	1	h	h	NOUN
eurjchem-365	51	2	n	n	ADP
eurjchem-365	51	3	h	h	NOUN
eurjchem-365	51	4	n	n	CCONJ
eurjchem-365	51	5	ph	ph	ADJ
eurjchem-365	51	6	pocl3	pocl3	NOUN
eurjchem-365	51	7	pocl3	pocl3	NOUN
eurjchem-365	51	8	o	o	NOUN
eurjchem-365	51	9	n	n	ADP
eurjchem-365	51	10	ar	ar	PROPN
eurjchem-365	51	11	n	n	ADP
eurjchem-365	51	12	o	o	NOUN
eurjchem-365	51	13	n	n	X
eurjchem-365	51	14	phar	phar	X
eurjchem-365	51	15	(	(	PUNCT
eurjchem-365	51	16	16	16	NUM
eurjchem-365	51	17	)	)	PUNCT
eurjchem-365	51	18	(	(	PUNCT
eurjchem-365	51	19	18	18	NUM
eurjchem-365	51	20	)	)	PUNCT
eurjchem-365	51	21	(	(	PUNCT
eurjchem-365	51	22	20	20	NUM
eurjchem-365	51	23	)	)	PUNCT
eurjchem-365	51	24	(	(	PUNCT
eurjchem-365	51	25	21	21	NUM
eurjchem-365	51	26	)	)	PUNCT
eurjchem-365	51	27	(	(	PUNCT
eurjchem-365	51	28	19	19	NUM
eurjchem-365	51	29	)	)	PUNCT
eurjchem-365	51	30	(	(	PUNCT
eurjchem-365	51	31	-h2o	-h2o	NOUN
eurjchem-365	51	32	)	)	PUNCT
eurjchem-365	51	33	(	(	PUNCT
eurjchem-365	51	34	-h2o	-h2o	NOUN
eurjchem-365	51	35	)	)	PUNCT
eurjchem-365	51	36	nh2	nh2	NOUN
eurjchem-365	52	1	sh	sh	INTJ
eurjchem-365	52	2	s	s	VERB
eurjchem-365	53	1	hn	hn	PROPN
eurjchem-365	53	2	o	o	PROPN
eurjchem-365	53	3	cnph	cnph	ADJ
eurjchem-365	53	4	(	(	PUNCT
eurjchem-365	53	5	17	17	NUM
eurjchem-365	53	6	)	)	PUNCT
eurjchem-365	53	7	4	4	NUM
eurjchem-365	53	8	)	)	PUNCT
eurjchem-365	53	9	r	r	NOUN
eurjchem-365	53	10	=	=	PUNCT
eurjchem-365	53	11	c6h4	c6h4	NOUN
eurjchem-365	53	12	-	-	NOUN
eurjchem-365	53	13	oh	oh	INTJ
eurjchem-365	53	14	(	(	PUNCT
eurjchem-365	53	15	4	4	NUM
eurjchem-365	53	16	)	)	PUNCT
eurjchem-365	53	17	ar	ar	NOUN
eurjchem-365	53	18	c	c	NOUN
eurjchem-365	53	19	o	o	NOUN
eurjchem-365	53	20	h	h	NOUN
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eurjchem-365	53	22	r	r	NOUN
eurjchem-365	53	23	ph	ph	NOUN
eurjchem-365	53	24	scheme	scheme	NOUN
eurjchem-365	53	25	1	1	NUM
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eurjchem-365	53	31	/	/	SYM
eurjchem-365	53	32	european	european	PROPN
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eurjchem-365	53	39	)	)	PUNCT
eurjchem-365	53	40	(	(	PUNCT
eurjchem-365	53	41	2011	2011	NUM
eurjchem-365	53	42	)	)	PUNCT
eurjchem-365	53	43	200‐205	200‐205	NUM
eurjchem-365	53	44	1h	1h	NUM
eurjchem-365	53	45	nmr	nmr	NOUN
eurjchem-365	53	46	(	(	PUNCT
eurjchem-365	53	47	300	300	NUM
eurjchem-365	53	48	mhz	mhz	NOUN
eurjchem-365	53	49	,	,	PUNCT
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eurjchem-365	53	51	):	):	PUNCT
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eurjchem-365	53	53	(	(	PUNCT
eurjchem-365	53	54	s	s	PROPN
eurjchem-365	53	55	,	,	PUNCT
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eurjchem-365	53	57	,	,	PUNCT
eurjchem-365	53	58	och3	och3	ADJ
eurjchem-365	53	59	)	)	PUNCT
eurjchem-365	53	60	,	,	PUNCT
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eurjchem-365	53	69	)	)	PUNCT
eurjchem-365	53	70	,	,	PUNCT
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eurjchem-365	53	74	,	,	PUNCT
eurjchem-365	53	75	1h	1h	NUM
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eurjchem-365	53	77	=	=	NOUN
eurjchem-365	53	78	ch	ch	NOUN
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eurjchem-365	53	80	,	,	PUNCT
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eurjchem-365	53	82	(	(	PUNCT
eurjchem-365	53	83	s	s	PROPN
eurjchem-365	53	84	,	,	PUNCT
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eurjchem-365	53	86	,	,	PUNCT
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eurjchem-365	54	1	ms	ms	NOUN
eurjchem-365	54	2	(	(	PUNCT
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eurjchem-365	54	4	,	,	PUNCT
eurjchem-365	54	5	m	m	PROPN
eurjchem-365	54	6	/	/	SYM
eurjchem-365	54	7	z	z	NOUN
eurjchem-365	54	8	):	):	PUNCT
eurjchem-365	54	9	278(m.+	278(m.+	NUM
eurjchem-365	54	10	)	)	PUNCT
eurjchem-365	54	11	.	.	PUNCT
eurjchem-365	55	1	anal	anal	PROPN
eurjchem-365	55	2	.	.	PUNCT
eurjchem-365	55	3	calcd	calcd	NOUN
eurjchem-365	55	4	.	.	PUNCT
eurjchem-365	56	1	for	for	SCONJ
eurjchem-365	56	2	c17h14n2o2	c17h14n2o2	NOUN
eurjchem-365	56	3	:	:	PUNCT
eurjchem-365	56	4	c	c	NOUN
eurjchem-365	56	5	,	,	PUNCT
eurjchem-365	56	6	73.38	73.38	NUM
eurjchem-365	56	7	;	;	PUNCT
eurjchem-365	56	8	h	h	NOUN
eurjchem-365	56	9	,	,	PUNCT
eurjchem-365	56	10	5.03	5.03	NUM
eurjchem-365	56	11	;	;	PUNCT
eurjchem-365	56	12	n	n	CCONJ
eurjchem-365	56	13	,	,	PUNCT
eurjchem-365	56	14	10.07	10.07	NUM
eurjchem-365	56	15	.	.	PUNCT
eurjchem-365	56	16	found	find	VERB
eurjchem-365	56	17	:	:	PUNCT
eurjchem-365	57	1	c	c	X
eurjchem-365	57	2	,	,	PUNCT
eurjchem-365	57	3	73.11	73.11	NUM
eurjchem-365	57	4	;	;	PUNCT
eurjchem-365	57	5	h	h	NOUN
eurjchem-365	57	6	,	,	PUNCT
eurjchem-365	57	7	5.41	5.41	NUM
eurjchem-365	57	8	;	;	PUNCT
eurjchem-365	57	9	n	n	CCONJ
eurjchem-365	57	10	,	,	PUNCT
eurjchem-365	57	11	10.32	10.32	NUM
eurjchem-365	57	12	%	%	NOUN
eurjchem-365	57	13	.	.	PUNCT
eurjchem-365	58	1	2.3	2.3	NUM
eurjchem-365	58	2	.	.	PUNCT
eurjchem-365	58	3	n‐(4‐hydroxyphenyl	n‐(4‐hydroxyphenyl	NUM
eurjchem-365	58	4	)	)	PUNCT
eurjchem-365	58	5	2‐cyano‐3‐phenyl‐2‐propenoyl	2‐cyano‐3‐phenyl‐2‐propenoyl	NOUN
eurjchem-365	58	6	amide	amide	NOUN
eurjchem-365	58	7	(	(	PUNCT
eurjchem-365	58	8	4	4	NUM
eurjchem-365	58	9	)	)	PUNCT
eurjchem-365	58	10	a	a	DET
eurjchem-365	58	11	mixture	mixture	NOUN
eurjchem-365	58	12	of	of	ADP
eurjchem-365	58	13	3	3	NUM
eurjchem-365	58	14	(	(	PUNCT
eurjchem-365	58	15	1.4	1.4	NUM
eurjchem-365	58	16	g	g	NOUN
eurjchem-365	58	17	,	,	PUNCT
eurjchem-365	58	18	5	5	NUM
eurjchem-365	58	19	mmol	mmol	NOUN
eurjchem-365	58	20	)	)	PUNCT
eurjchem-365	58	21	and	and	CCONJ
eurjchem-365	58	22	anhydrous	anhydrous	ADJ
eurjchem-365	58	23	aluminium	aluminium	NOUN
eurjchem-365	58	24	chloride	chloride	NOUN
eurjchem-365	58	25	(	(	PUNCT
eurjchem-365	58	26	1.33	1.33	NUM
eurjchem-365	58	27	g	g	NOUN
eurjchem-365	58	28	,	,	PUNCT
eurjchem-365	58	29	10	10	NUM
eurjchem-365	58	30	mmol	mmol	NOUN
eurjchem-365	58	31	)	)	PUNCT
eurjchem-365	58	32	in	in	ADP
eurjchem-365	58	33	dry	dry	ADJ
eurjchem-365	58	34	benzene	benzene	NOUN
eurjchem-365	58	35	or	or	CCONJ
eurjchem-365	58	36	chlorobenzene	chlorobenzene	NOUN
eurjchem-365	58	37	(	(	PUNCT
eurjchem-365	58	38	50	50	NUM
eurjchem-365	58	39	ml	ml	NOUN
eurjchem-365	58	40	)	)	PUNCT
eurjchem-365	58	41	was	be	AUX
eurjchem-365	58	42	stirred	stir	VERB
eurjchem-365	58	43	at	at	ADP
eurjchem-365	58	44	room	room	NOUN
eurjchem-365	58	45	temperature	temperature	NOUN
eurjchem-365	58	46	for	for	ADP
eurjchem-365	58	47	three	three	NUM
eurjchem-365	58	48	hours	hour	NOUN
eurjchem-365	58	49	,	,	PUNCT
eurjchem-365	58	50	then	then	ADV
eurjchem-365	58	51	refluxed	refluxe	VERB
eurjchem-365	58	52	for	for	ADP
eurjchem-365	58	53	24	24	NUM
eurjchem-365	58	54	hours	hour	NOUN
eurjchem-365	58	55	and	and	CCONJ
eurjchem-365	58	56	left	leave	VERB
eurjchem-365	58	57	overnight	overnight	ADV
eurjchem-365	58	58	.	.	PUNCT
eurjchem-365	59	1	the	the	DET
eurjchem-365	59	2	reaction	reaction	NOUN
eurjchem-365	59	3	mixture	mixture	NOUN
eurjchem-365	59	4	was	be	AUX
eurjchem-365	59	5	poured	pour	VERB
eurjchem-365	59	6	onto	onto	ADP
eurjchem-365	59	7	cold	cold	ADJ
eurjchem-365	59	8	dilute	dilute	NOUN
eurjchem-365	59	9	hcl	hcl	PROPN
eurjchem-365	59	10	.	.	PUNCT
eurjchem-365	60	1	the	the	DET
eurjchem-365	60	2	organic	organic	ADJ
eurjchem-365	60	3	solvent	solvent	NOUN
eurjchem-365	60	4	was	be	AUX
eurjchem-365	60	5	removed	remove	VERB
eurjchem-365	60	6	by	by	ADP
eurjchem-365	60	7	steam	steam	NOUN
eurjchem-365	60	8	distillation	distillation	NOUN
eurjchem-365	60	9	and	and	CCONJ
eurjchem-365	60	10	the	the	DET
eurjchem-365	60	11	residue	residue	NOUN
eurjchem-365	60	12	was	be	AUX
eurjchem-365	60	13	extracted	extract	VERB
eurjchem-365	60	14	by	by	ADP
eurjchem-365	60	15	diethyl	diethyl	NOUN
eurjchem-365	60	16	ether	ether	NOUN
eurjchem-365	60	17	(	(	PUNCT
eurjchem-365	60	18	3	3	NUM
eurjchem-365	60	19	x	x	SYM
eurjchem-365	60	20	50	50	NUM
eurjchem-365	60	21	ml	ml	NOUN
eurjchem-365	60	22	)	)	PUNCT
eurjchem-365	60	23	,	,	PUNCT
eurjchem-365	60	24	and	and	CCONJ
eurjchem-365	60	25	then	then	ADV
eurjchem-365	60	26	dried	dry	VERB
eurjchem-365	60	27	over	over	ADP
eurjchem-365	60	28	anhydrous	anhydrous	ADJ
eurjchem-365	60	29	mgso4	mgso4	PROPN
eurjchem-365	60	30	.	.	PUNCT
eurjchem-365	61	1	the	the	DET
eurjchem-365	61	2	diethyl	diethyl	NOUN
eurjchem-365	61	3	ether	ether	NOUN
eurjchem-365	61	4	was	be	AUX
eurjchem-365	61	5	removed	remove	VERB
eurjchem-365	61	6	by	by	ADP
eurjchem-365	61	7	distillation	distillation	NOUN
eurjchem-365	61	8	and	and	CCONJ
eurjchem-365	61	9	the	the	DET
eurjchem-365	61	10	residue	residue	NOUN
eurjchem-365	61	11	was	be	AUX
eurjchem-365	61	12	crystallized	crystallize	VERB
eurjchem-365	61	13	from	from	ADP
eurjchem-365	61	14	methanol	methanol	NOUN
eurjchem-365	61	15	to	to	PART
eurjchem-365	61	16	give	give	VERB
eurjchem-365	61	17	4	4	NUM
eurjchem-365	61	18	as	as	ADP
eurjchem-365	61	19	green	green	ADJ
eurjchem-365	61	20	crystals	crystal	NOUN
eurjchem-365	61	21	(	(	PUNCT
eurjchem-365	61	22	scheme	scheme	NOUN
eurjchem-365	61	23	1	1	NUM
eurjchem-365	61	24	)	)	PUNCT
eurjchem-365	61	25	.	.	PUNCT
eurjchem-365	62	1	yield	yield	NOUN
eurjchem-365	62	2	:	:	PUNCT
eurjchem-365	62	3	90‐95	90‐95	NUM
eurjchem-365	62	4	%	%	NOUN
eurjchem-365	62	5	.	.	PUNCT
eurjchem-365	63	1	m.p	m.p	PROPN
eurjchem-365	63	2	.	.	PROPN
eurjchem-365	63	3	:	:	PUNCT
eurjchem-365	64	1	195‐196	195‐196	NUM
eurjchem-365	64	2	oc	oc	X
eurjchem-365	64	3	.	.	PUNCT
eurjchem-365	64	4	ft‐ir	ft‐ir	NOUN
eurjchem-365	64	5	(	(	PUNCT
eurjchem-365	64	6	kbr	kbr	PROPN
eurjchem-365	64	7	,	,	PUNCT
eurjchem-365	64	8	cm‐1	cm‐1	PROPN
eurjchem-365	64	9	):	):	PUNCT
eurjchem-365	64	10	3338	3338	NUM
eurjchem-365	64	11	,	,	PUNCT
eurjchem-365	64	12	3258	3258	NUM
eurjchem-365	64	13	(nh	(nh	NOUN
eurjchem-365	64	14	)	)	PUNCT
eurjchem-365	64	15	,	,	PUNCT
eurjchem-365	64	16	2222	2222	NUM
eurjchem-365	64	17	(cn	(cn	NOUN
eurjchem-365	64	18	)	)	PUNCT
eurjchem-365	64	19	,	,	PUNCT
eurjchem-365	64	20	1653	1653	NUM
eurjchem-365	64	21	(c	(c	NOUN
eurjchem-365	64	22	=	=	SYM
eurjchem-365	64	23	o	o	NOUN
eurjchem-365	64	24	)	)	PUNCT
eurjchem-365	64	25	(	(	PUNCT
eurjchem-365	64	26	amide	amide	NOUN
eurjchem-365	64	27	)	)	PUNCT
eurjchem-365	64	28	.	.	PUNCT
eurjchem-365	65	1	1h	1h	NUM
eurjchem-365	65	2	nmr	nmr	NOUN
eurjchem-365	65	3	(	(	PUNCT
eurjchem-365	65	4	300	300	NUM
eurjchem-365	65	5	mhz	mhz	NOUN
eurjchem-365	65	6	,	,	PUNCT
eurjchem-365	65	7	dmso‐d6	dmso‐d6	NUM
eurjchem-365	65	8	):	):	PUNCT
eurjchem-365	65	9	6.75‐7.96	6.75‐7.96	PROPN
eurjchem-365	65	10	(	(	PUNCT
eurjchem-365	65	11	m	m	PROPN
eurjchem-365	65	12	,	,	PUNCT
eurjchem-365	65	13	9	9	NUM
eurjchem-365	65	14	h	h	NOUN
eurjchem-365	65	15	,	,	PUNCT
eurjchem-365	65	16	ar‐	ar‐	PROPN
eurjchem-365	65	17	h	h	NOUN
eurjchem-365	65	18	)	)	PUNCT
eurjchem-365	65	19	,	,	PUNCT
eurjchem-365	65	20	8.22	8.22	NUM
eurjchem-365	65	21	(	(	PUNCT
eurjchem-365	65	22	s	s	PROPN
eurjchem-365	65	23	,	,	PUNCT
eurjchem-365	65	24	1h	1h	NUM
eurjchem-365	65	25	,	,	PUNCT
eurjchem-365	65	26	=	=	NOUN
eurjchem-365	65	27	ch	ch	NOUN
eurjchem-365	65	28	)	)	PUNCT
eurjchem-365	65	29	,	,	PUNCT
eurjchem-365	65	30	9.36	9.36	NUM
eurjchem-365	65	31	(	(	PUNCT
eurjchem-365	65	32	s	s	PROPN
eurjchem-365	65	33	,	,	PUNCT
eurjchem-365	65	34	1h	1h	NUM
eurjchem-365	65	35	,	,	PUNCT
eurjchem-365	65	36	nh	nh	PROPN
eurjchem-365	65	37	)	)	PUNCT
eurjchem-365	65	38	,	,	PUNCT
eurjchem-365	65	39	10.14	10.14	NUM
eurjchem-365	65	40	(	(	PUNCT
eurjchem-365	65	41	s	s	PROPN
eurjchem-365	65	42	,	,	PUNCT
eurjchem-365	65	43	1h	1h	NUM
eurjchem-365	65	44	,	,	PUNCT
eurjchem-365	65	45	oh	oh	INTJ
eurjchem-365	65	46	)	)	PUNCT
eurjchem-365	65	47	.	.	PUNCT
eurjchem-365	66	1	ms	ms	NOUN
eurjchem-365	66	2	(	(	PUNCT
eurjchem-365	66	3	ei	ei	PROPN
eurjchem-365	66	4	,	,	PUNCT
eurjchem-365	66	5	m	m	PROPN
eurjchem-365	66	6	/	/	SYM
eurjchem-365	66	7	z	z	ADJ
eurjchem-365	66	8	):	):	PUNCT
eurjchem-365	66	9	264	264	NUM
eurjchem-365	66	10	(	(	PUNCT
eurjchem-365	66	11	m+	m+	NUM
eurjchem-365	66	12	)	)	PUNCT
eurjchem-365	66	13	.	.	PUNCT
eurjchem-365	67	1	anal	anal	PROPN
eurjchem-365	67	2	.	.	PUNCT
eurjchem-365	67	3	calcd	calcd	NOUN
eurjchem-365	67	4	.	.	PUNCT
eurjchem-365	68	1	for	for	ADP
eurjchem-365	68	2	c16h12n2o2	c16h12n2o2	NOUN
eurjchem-365	68	3	:	:	PUNCT
eurjchem-365	68	4	c	c	NOUN
eurjchem-365	68	5	,	,	PUNCT
eurjchem-365	68	6	72.72	72.72	NUM
eurjchem-365	68	7	;	;	PUNCT
eurjchem-365	68	8	h	h	NOUN
eurjchem-365	68	9	,	,	PUNCT
eurjchem-365	68	10	4.54	4.54	NUM
eurjchem-365	68	11	;	;	PUNCT
eurjchem-365	68	12	n	n	CCONJ
eurjchem-365	68	13	,	,	PUNCT
eurjchem-365	68	14	10.61	10.61	NUM
eurjchem-365	68	15	.	.	PUNCT
eurjchem-365	68	16	found	find	VERB
eurjchem-365	68	17	:	:	PUNCT
eurjchem-365	69	1	c	c	X
eurjchem-365	69	2	,	,	PUNCT
eurjchem-365	69	3	73.00	73.00	NUM
eurjchem-365	69	4	;	;	PUNCT
eurjchem-365	69	5	h	h	X
eurjchem-365	69	6	,	,	PUNCT
eurjchem-365	69	7	4.42	4.42	NUM
eurjchem-365	69	8	;	;	PUNCT
eurjchem-365	69	9	n	n	CCONJ
eurjchem-365	69	10	,	,	PUNCT
eurjchem-365	69	11	10.31	10.31	NUM
eurjchem-365	69	12	%	%	NOUN
eurjchem-365	69	13	.	.	PUNCT
eurjchem-365	70	1	2.4	2.4	NUM
eurjchem-365	70	2	.	.	PUNCT
eurjchem-365	70	3	general	general	ADJ
eurjchem-365	70	4	procedure	procedure	NOUN
eurjchem-365	70	5	to	to	PART
eurjchem-365	70	6	synthesize	synthesize	VERB
eurjchem-365	70	7	compounds	compound	NOUN
eurjchem-365	70	8	5	5	NUM
eurjchem-365	70	9	,	,	PUNCT
eurjchem-365	70	10	6	6	NUM
eurjchem-365	70	11	,	,	PUNCT
eurjchem-365	70	12	7	7	NUM
eurjchem-365	70	13	,	,	PUNCT
eurjchem-365	70	14	8	8	NUM
eurjchem-365	70	15	,	,	PUNCT
eurjchem-365	70	16	9	9	NUM
eurjchem-365	70	17	,	,	PUNCT
eurjchem-365	70	18	17	17	NUM
eurjchem-365	70	19	,	,	PUNCT
eurjchem-365	70	20	18	18	NUM
eurjchem-365	70	21	and	and	CCONJ
eurjchem-365	70	22	20	20	NUM
eurjchem-365	70	23	to	to	ADP
eurjchem-365	70	24	a	a	DET
eurjchem-365	70	25	solution	solution	NOUN
eurjchem-365	70	26	of	of	ADP
eurjchem-365	70	27	propenoyl	propenoyl	PROPN
eurjchem-365	70	28	chloride	chloride	NOUN
eurjchem-365	70	29	(	(	PUNCT
eurjchem-365	70	30	1	1	NUM
eurjchem-365	70	31	)	)	PUNCT
eurjchem-365	70	32	(	(	PUNCT
eurjchem-365	70	33	1.9	1.9	NUM
eurjchem-365	70	34	g	g	NOUN
eurjchem-365	70	35	;	;	PUNCT
eurjchem-365	70	36	10	10	NUM
eurjchem-365	70	37	mmol	mmol	NOUN
eurjchem-365	70	38	)	)	PUNCT
eurjchem-365	70	39	in	in	ADP
eurjchem-365	70	40	dry	dry	ADJ
eurjchem-365	70	41	benzene	benzene	NOUN
eurjchem-365	70	42	(	(	PUNCT
eurjchem-365	70	43	30	30	NUM
eurjchem-365	70	44	ml	ml	NOUN
eurjchem-365	70	45	)	)	PUNCT
eurjchem-365	70	46	containing	contain	VERB
eurjchem-365	70	47	triethylamine	triethylamine	NOUN
eurjchem-365	70	48	(	(	PUNCT
eurjchem-365	70	49	1.38	1.38	NUM
eurjchem-365	70	50	ml	ml	NOUN
eurjchem-365	70	51	;	;	PUNCT
eurjchem-365	70	52	10	10	NUM
eurjchem-365	70	53	mmol	mmol	NOUN
eurjchem-365	70	54	)	)	PUNCT
eurjchem-365	70	55	,	,	PUNCT
eurjchem-365	70	56	o‐cresol	o‐cresol	X
eurjchem-365	70	57	,	,	PUNCT
eurjchem-365	70	58	p‐thiocresol	p‐thiocresol	X
eurjchem-365	70	59	,	,	PUNCT
eurjchem-365	70	60	ethanolamine	ethanolamine	NOUN
eurjchem-365	70	61	,	,	PUNCT
eurjchem-365	70	62	o‐phenylene	o‐phenylene	ADV
eurjchem-365	70	63	diamine	diamine	NOUN
eurjchem-365	70	64	,	,	PUNCT
eurjchem-365	70	65	anthranilic	anthranilic	NOUN
eurjchem-365	70	66	acid	acid	NOUN
eurjchem-365	70	67	,	,	PUNCT
eurjchem-365	70	68	2‐aminothiophenol	2‐aminothiophenol	NUM
eurjchem-365	70	69	,	,	PUNCT
eurjchem-365	70	70	benzoyl	benzoyl	ADJ
eurjchem-365	70	71	hydrazine	hydrazine	NOUN
eurjchem-365	70	72	and/or	and/or	CCONJ
eurjchem-365	70	73	2‐aminophenol	2‐aminophenol	NUM
eurjchem-365	70	74	(	(	PUNCT
eurjchem-365	70	75	10	10	NUM
eurjchem-365	70	76	mmol	mmol	NOUN
eurjchem-365	70	77	)	)	PUNCT
eurjchem-365	70	78	was	be	AUX
eurjchem-365	70	79	added	add	VERB
eurjchem-365	70	80	and	and	CCONJ
eurjchem-365	70	81	the	the	DET
eurjchem-365	70	82	reaction	reaction	NOUN
eurjchem-365	70	83	mixture	mixture	NOUN
eurjchem-365	70	84	was	be	AUX
eurjchem-365	70	85	stirred	stir	VERB
eurjchem-365	70	86	at	at	ADP
eurjchem-365	70	87	room	room	NOUN
eurjchem-365	70	88	temperature	temperature	NOUN
eurjchem-365	70	89	for	for	ADP
eurjchem-365	70	90	1	1	NUM
eurjchem-365	70	91	h.	h.	NOUN
eurjchem-365	70	92	the	the	DET
eurjchem-365	70	93	triethylamine	triethylamine	NOUN
eurjchem-365	70	94	hydrochloride	hydrochloride	NOUN
eurjchem-365	70	95	was	be	AUX
eurjchem-365	70	96	filtered	filter	VERB
eurjchem-365	70	97	off	off	ADP
eurjchem-365	70	98	and	and	CCONJ
eurjchem-365	70	99	most	most	ADJ
eurjchem-365	70	100	of	of	ADP
eurjchem-365	70	101	the	the	DET
eurjchem-365	70	102	solvent	solvent	NOUN
eurjchem-365	70	103	was	be	AUX
eurjchem-365	70	104	distilled	distil	VERB
eurjchem-365	70	105	off	off	ADP
eurjchem-365	70	106	.	.	PUNCT
eurjchem-365	71	1	the	the	DET
eurjchem-365	71	2	solid	solid	ADJ
eurjchem-365	71	3	that	that	PRON
eurjchem-365	71	4	separated	separate	VERB
eurjchem-365	71	5	out	out	ADP
eurjchem-365	71	6	was	be	AUX
eurjchem-365	71	7	collected	collect	VERB
eurjchem-365	71	8	by	by	ADP
eurjchem-365	71	9	suction	suction	NOUN
eurjchem-365	71	10	and	and	CCONJ
eurjchem-365	71	11	recrystallized	recrystallize	VERB
eurjchem-365	71	12	from	from	ADP
eurjchem-365	71	13	the	the	DET
eurjchem-365	71	14	appropriate	appropriate	ADJ
eurjchem-365	71	15	solvent	solvent	NOUN
eurjchem-365	71	16	to	to	PART
eurjchem-365	71	17	afford	afford	VERB
eurjchem-365	71	18	the	the	DET
eurjchem-365	71	19	desired	desire	VERB
eurjchem-365	71	20	product	product	NOUN
eurjchem-365	71	21	(	(	PUNCT
eurjchem-365	71	22	scheme	scheme	NOUN
eurjchem-365	71	23	1	1	NUM
eurjchem-365	71	24	)	)	PUNCT
eurjchem-365	71	25	.	.	PUNCT
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eurjchem-365	72	2	2‐cyano‐3‐phenyl‐2‐propenoate	2‐cyano‐3‐phenyl‐2‐propenoate	NOUN
eurjchem-365	72	3	(	(	PUNCT
eurjchem-365	72	4	5	5	NUM
eurjchem-365	72	5	):	):	PUNCT
eurjchem-365	72	6	comp‐	comp‐	NOUN
eurjchem-365	72	7	ound	ound	ADV
eurjchem-365	72	8	5	5	NUM
eurjchem-365	72	9	crystallized	crystallize	VERB
eurjchem-365	72	10	from	from	ADP
eurjchem-365	72	11	benzene	benzene	NOUN
eurjchem-365	72	12	to	to	PART
eurjchem-365	72	13	give	give	VERB
eurjchem-365	72	14	green	green	ADJ
eurjchem-365	72	15	crystals	crystal	NOUN
eurjchem-365	72	16	.	.	PUNCT
eurjchem-365	73	1	yield	yield	NOUN
eurjchem-365	73	2	:	:	PUNCT
eurjchem-365	73	3	85	85	NUM
eurjchem-365	73	4	%	%	NOUN
eurjchem-365	73	5	.	.	PUNCT
eurjchem-365	74	1	m.p	m.p	PROPN
eurjchem-365	74	2	.	.	PROPN
eurjchem-365	74	3	:	:	PUNCT
eurjchem-365	75	1	101‐103	101‐103	NUM
eurjchem-365	75	2	oc	oc	PROPN
eurjchem-365	75	3	.	.	PUNCT
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eurjchem-365	75	5	(	(	PUNCT
eurjchem-365	75	6	kbr	kbr	PROPN
eurjchem-365	75	7	,	,	PUNCT
eurjchem-365	75	8	cm‐1	cm‐1	PROPN
eurjchem-365	75	9	):	):	PUNCT
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eurjchem-365	75	12	)	)	PUNCT
eurjchem-365	75	13	,	,	PUNCT
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eurjchem-365	75	15	(c	(c	NOUN
eurjchem-365	75	16	=	=	SYM
eurjchem-365	75	17	o	o	NOUN
eurjchem-365	75	18	)	)	PUNCT
eurjchem-365	75	19	(	(	PUNCT
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eurjchem-365	75	21	)	)	PUNCT
eurjchem-365	75	22	.	.	PUNCT
eurjchem-365	76	1	1h	1h	NUM
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eurjchem-365	76	3	(	(	PUNCT
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eurjchem-365	76	5	mhz	mhz	NOUN
eurjchem-365	76	6	,	,	PUNCT
eurjchem-365	76	7	dmso‐d6	dmso‐d6	NUM
eurjchem-365	76	8	):	):	PUNCT
eurjchem-365	76	9	2.20	2.20	NUM
eurjchem-365	76	10	(	(	PUNCT
eurjchem-365	76	11	s	s	PROPN
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eurjchem-365	76	15	ch3	ch3	PROPN
eurjchem-365	76	16	)	)	PUNCT
eurjchem-365	76	17	,	,	PUNCT
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eurjchem-365	76	19	(	(	PUNCT
eurjchem-365	76	20	m	m	PROPN
eurjchem-365	76	21	,	,	PUNCT
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eurjchem-365	77	8	):	):	PUNCT
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eurjchem-365	77	10	(	(	PUNCT
eurjchem-365	77	11	m+	m+	NUM
eurjchem-365	77	12	.	.	PUNCT
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eurjchem-365	78	4	.	.	PUNCT
eurjchem-365	79	1	for	for	SCONJ
eurjchem-365	79	2	c17h13no2	c17h13no2	PROPN
eurjchem-365	79	3	:	:	PUNCT
eurjchem-365	79	4	c	c	X
eurjchem-365	79	5	,	,	PUNCT
eurjchem-365	79	6	77.56	77.56	NUM
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eurjchem-365	79	8	h	h	NOUN
eurjchem-365	79	9	,	,	PUNCT
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eurjchem-365	79	12	n	n	CCONJ
eurjchem-365	79	13	,	,	PUNCT
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eurjchem-365	79	15	.	.	PUNCT
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eurjchem-365	79	17	:	:	PUNCT
eurjchem-365	80	1	c	c	X
eurjchem-365	80	2	,	,	PUNCT
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eurjchem-365	80	10	,	,	PUNCT
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eurjchem-365	80	13	.	.	PUNCT
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eurjchem-365	81	3	(	(	PUNCT
eurjchem-365	81	4	6	6	NUM
eurjchem-365	81	5	):	):	PUNCT
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eurjchem-365	81	7	6	6	NUM
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eurjchem-365	81	13	yellow	yellow	ADJ
eurjchem-365	81	14	crystals	crystal	NOUN
eurjchem-365	81	15	.	.	PUNCT
eurjchem-365	82	1	yield	yield	NOUN
eurjchem-365	82	2	:	:	PUNCT
eurjchem-365	82	3	90	90	NUM
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eurjchem-365	83	3	:	:	PUNCT
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eurjchem-365	84	5	(	(	PUNCT
eurjchem-365	84	6	kbr	kbr	PROPN
eurjchem-365	84	7	,	,	PUNCT
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eurjchem-365	84	9	):	):	PUNCT
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eurjchem-365	84	16	=	=	SYM
eurjchem-365	84	17	o	o	NOUN
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eurjchem-365	84	19	(	(	PUNCT
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eurjchem-365	84	21	)	)	PUNCT
eurjchem-365	84	22	.	.	PUNCT
eurjchem-365	85	1	1h	1h	NUM
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eurjchem-365	85	6	,	,	PUNCT
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eurjchem-365	85	8	):	):	PUNCT
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eurjchem-365	85	10	(	(	PUNCT
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eurjchem-365	85	17	,	,	PUNCT
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eurjchem-365	85	19	8.09	8.09	NUM
eurjchem-365	85	20	(	(	PUNCT
eurjchem-365	85	21	m	m	PROPN
eurjchem-365	85	22	,	,	PUNCT
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eurjchem-365	85	32	,	,	PUNCT
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eurjchem-365	86	2	(	(	PUNCT
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eurjchem-365	86	7	z	z	NOUN
eurjchem-365	86	8	):	):	PUNCT
eurjchem-365	86	9	279	279	NUM
eurjchem-365	86	10	(	(	PUNCT
eurjchem-365	86	11	m.+	m.+	NOUN
eurjchem-365	86	12	)	)	PUNCT
eurjchem-365	86	13	.	.	PUNCT
eurjchem-365	87	1	anal	anal	PROPN
eurjchem-365	87	2	.	.	PUNCT
eurjchem-365	87	3	calcd	calcd	NOUN
eurjchem-365	87	4	.	.	PUNCT
eurjchem-365	88	1	for	for	SCONJ
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eurjchem-365	88	3	:	:	PUNCT
eurjchem-365	88	4	c	c	X
eurjchem-365	88	5	,	,	PUNCT
eurjchem-365	88	6	73.11	73.11	NUM
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eurjchem-365	88	8	h	h	NOUN
eurjchem-365	88	9	,	,	PUNCT
eurjchem-365	88	10	4.65	4.65	NUM
eurjchem-365	88	11	;	;	PUNCT
eurjchem-365	88	12	n	n	CCONJ
eurjchem-365	88	13	,	,	PUNCT
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eurjchem-365	88	17	:	:	PUNCT
eurjchem-365	89	1	c	c	X
eurjchem-365	89	2	,	,	PUNCT
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eurjchem-365	89	4	;	;	PUNCT
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eurjchem-365	89	6	,	,	PUNCT
eurjchem-365	89	7	4.52	4.52	NUM
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eurjchem-365	89	13	.	.	PUNCT
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eurjchem-365	90	3	(	(	PUNCT
eurjchem-365	90	4	7	7	NUM
eurjchem-365	90	5	):	):	PUNCT
eurjchem-365	90	6	compound	compound	NOUN
eurjchem-365	90	7	7	7	NUM
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eurjchem-365	90	14	yellow	yellow	ADJ
eurjchem-365	90	15	crystals	crystal	NOUN
eurjchem-365	90	16	.	.	PUNCT
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eurjchem-365	91	2	:	:	PUNCT
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eurjchem-365	92	3	:	:	PUNCT
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eurjchem-365	92	5	oc	oc	X
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eurjchem-365	92	9	kbr	kbr	PROPN
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eurjchem-365	92	15	)	)	PUNCT
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eurjchem-365	92	19	)	)	PUNCT
eurjchem-365	92	20	,	,	PUNCT
eurjchem-365	92	21	1726	1726	NUM
eurjchem-365	92	22	(c	(c	NOUN
eurjchem-365	92	23	=	=	SYM
eurjchem-365	92	24	o	o	NOUN
eurjchem-365	92	25	)	)	PUNCT
eurjchem-365	92	26	(	(	PUNCT
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eurjchem-365	92	28	)	)	PUNCT
eurjchem-365	92	29	,	,	PUNCT
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eurjchem-365	92	31	(c	(c	PROPN
eurjchem-365	92	32	=	=	SYM
eurjchem-365	92	33	o	o	NOUN
eurjchem-365	92	34	)	)	PUNCT
eurjchem-365	92	35	(	(	PUNCT
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eurjchem-365	92	37	)	)	PUNCT
eurjchem-365	92	38	.	.	PUNCT
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eurjchem-365	93	8	):	):	PUNCT
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eurjchem-365	93	11	q	q	NOUN
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eurjchem-365	93	21	,	,	PUNCT
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eurjchem-365	93	23	,	,	PUNCT
eurjchem-365	93	24	ch2‐o	ch2‐o	NOUN
eurjchem-365	93	25	)	)	PUNCT
eurjchem-365	93	26	,	,	PUNCT
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eurjchem-365	93	34	)	)	PUNCT
eurjchem-365	93	35	,	,	PUNCT
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eurjchem-365	93	39	,	,	PUNCT
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eurjchem-365	93	45	,	,	PUNCT
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eurjchem-365	93	55	,	,	PUNCT
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eurjchem-365	94	17	.	.	PUNCT
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eurjchem-365	95	2	.	.	PUNCT
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eurjchem-365	95	4	.	.	PUNCT
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eurjchem-365	96	5	,	,	PUNCT
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eurjchem-365	96	7	;	;	PUNCT
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eurjchem-365	96	9	,	,	PUNCT
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eurjchem-365	96	13	,	,	PUNCT
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eurjchem-365	96	17	:	:	PUNCT
eurjchem-365	97	1	c	c	X
eurjchem-365	97	2	,	,	PUNCT
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eurjchem-365	97	6	,	,	PUNCT
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eurjchem-365	97	8	;	;	PUNCT
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eurjchem-365	97	10	,	,	PUNCT
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eurjchem-365	98	3	,	,	PUNCT
eurjchem-365	98	4	n'‐(1,2‐phenylene)bis(2‐cyano‐3‐phenylacryl	n'‐(1,2‐phenylene)bis(2‐cyano‐3‐phenylacryl	NOUN
eurjchem-365	98	5	amide	amide	NOUN
eurjchem-365	98	6	)	)	PUNCT
eurjchem-365	98	7	(	(	PUNCT
eurjchem-365	98	8	8)	8)	NUM
eurjchem-365	98	9	:	:	PUNCT
eurjchem-365	98	10	compound	compound	NOUN
eurjchem-365	98	11	8	8	NUM
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eurjchem-365	98	13	from	from	ADP
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eurjchem-365	98	19	.	.	PUNCT
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eurjchem-365	99	2	:	:	PUNCT
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eurjchem-365	100	3	:	:	PUNCT
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eurjchem-365	101	3	.	.	PUNCT
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eurjchem-365	101	5	(	(	PUNCT
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eurjchem-365	101	7	,	,	PUNCT
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eurjchem-365	101	12	)	)	PUNCT
eurjchem-365	101	13	,	,	PUNCT
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eurjchem-365	101	16	)	)	PUNCT
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eurjchem-365	101	19	(c	(c	PROPN
eurjchem-365	101	20	=	=	SYM
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eurjchem-365	101	22	)	)	PUNCT
eurjchem-365	101	23	(	(	PUNCT
eurjchem-365	101	24	amide	amide	NOUN
eurjchem-365	101	25	)	)	PUNCT
eurjchem-365	101	26	.	.	PUNCT
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eurjchem-365	102	3	(	(	PUNCT
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eurjchem-365	102	6	,	,	PUNCT
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eurjchem-365	102	8	):	):	PUNCT
eurjchem-365	102	9	7.32‐7.98	7.32‐7.98	NUM
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eurjchem-365	102	17	)	)	PUNCT
eurjchem-365	102	18	,	,	PUNCT
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eurjchem-365	103	8	):	):	PUNCT
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eurjchem-365	103	10	(	(	PUNCT
eurjchem-365	103	11	m.+	m.+	NOUN
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eurjchem-365	103	13	.	.	PUNCT
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eurjchem-365	104	4	.	.	PUNCT
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eurjchem-365	105	5	,	,	PUNCT
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eurjchem-365	105	9	,	,	PUNCT
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eurjchem-365	105	11	;	;	PUNCT
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eurjchem-365	105	13	,	,	PUNCT
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eurjchem-365	105	17	:	:	PUNCT
eurjchem-365	106	1	c	c	X
eurjchem-365	106	2	,	,	PUNCT
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eurjchem-365	107	2	acid	acid	NOUN
eurjchem-365	107	3	(	(	PUNCT
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eurjchem-365	107	5	):	):	PUNCT
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eurjchem-365	107	11	/	/	SYM
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eurjchem-365	107	17	.	.	PUNCT
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eurjchem-365	108	2	:	:	PUNCT
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eurjchem-365	112	8	):	):	PUNCT
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eurjchem-365	112	10	(	(	PUNCT
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eurjchem-365	114	5	,	,	PUNCT
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eurjchem-365	114	17	:	:	PUNCT
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eurjchem-365	117	2	:	:	PUNCT
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eurjchem-365	119	13	,	,	PUNCT
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eurjchem-365	119	17	,	,	PUNCT
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eurjchem-365	119	20	=	=	SYM
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eurjchem-365	119	23	(	(	PUNCT
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eurjchem-365	120	14	,	,	PUNCT
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eurjchem-365	120	16	=	=	SYM
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eurjchem-365	120	19	,	,	PUNCT
eurjchem-365	120	20	‐ch‐cn	‐ch‐cn	ADJ
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eurjchem-365	120	22	,	,	PUNCT
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eurjchem-365	120	26	,	,	PUNCT
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eurjchem-365	120	28	,	,	PUNCT
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eurjchem-365	120	30	=	=	SYM
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eurjchem-365	120	33	,	,	PUNCT
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eurjchem-365	120	36	,	,	PUNCT
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eurjchem-365	120	45	,	,	PUNCT
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eurjchem-365	120	52	nh	nh	PROPN
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eurjchem-365	120	54	.	.	PUNCT
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eurjchem-365	121	4	,	,	PUNCT
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eurjchem-365	121	8	):	):	PUNCT
eurjchem-365	121	9	280	280	NUM
eurjchem-365	121	10	(	(	PUNCT
eurjchem-365	121	11	m.+	m.+	NOUN
eurjchem-365	121	12	)	)	PUNCT
eurjchem-365	121	13	.	.	PUNCT
eurjchem-365	122	1	anal	anal	PROPN
eurjchem-365	122	2	.	.	PUNCT
eurjchem-365	122	3	calcd	calcd	NOUN
eurjchem-365	122	4	.	.	PUNCT
eurjchem-365	123	1	for	for	ADP
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eurjchem-365	123	4	c	c	X
eurjchem-365	123	5	,	,	PUNCT
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eurjchem-365	123	8	h	h	NOUN
eurjchem-365	123	9	,	,	PUNCT
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eurjchem-365	123	11	;	;	PUNCT
eurjchem-365	123	12	n	n	CCONJ
eurjchem-365	123	13	,	,	PUNCT
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eurjchem-365	123	17	:	:	PUNCT
eurjchem-365	124	1	c	c	X
eurjchem-365	124	2	,	,	PUNCT
eurjchem-365	124	3	69.38	69.38	NUM
eurjchem-365	124	4	;	;	PUNCT
eurjchem-365	124	5	h	h	NOUN
eurjchem-365	124	6	,	,	PUNCT
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eurjchem-365	124	8	;	;	PUNCT
eurjchem-365	124	9	n	n	CCONJ
eurjchem-365	124	10	,	,	PUNCT
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eurjchem-365	124	13	.	.	PUNCT
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eurjchem-365	125	2	(	(	PUNCT
eurjchem-365	125	3	18	18	NUM
eurjchem-365	125	4	):	):	PUNCT
eurjchem-365	125	5	compound	compound	NOUN
eurjchem-365	125	6	18	18	NUM
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eurjchem-365	125	8	from	from	ADP
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eurjchem-365	125	10	/	/	SYM
eurjchem-365	125	11	ethanol	ethanol	NOUN
eurjchem-365	125	12	to	to	PART
eurjchem-365	125	13	give	give	VERB
eurjchem-365	125	14	colourless	colourless	ADJ
eurjchem-365	125	15	crystals	crystal	NOUN
eurjchem-365	125	16	.	.	PUNCT
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eurjchem-365	126	2	:	:	PUNCT
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eurjchem-365	126	5	.	.	PUNCT
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eurjchem-365	127	3	:	:	PUNCT
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eurjchem-365	128	2	oc	oc	PROPN
eurjchem-365	128	3	.	.	PUNCT
eurjchem-365	128	4	ft‐ir	ft‐ir	NOUN
eurjchem-365	128	5	(	(	PUNCT
eurjchem-365	128	6	kbr	kbr	PROPN
eurjchem-365	128	7	,	,	PUNCT
eurjchem-365	128	8	cm‐1	cm‐1	PROPN
eurjchem-365	128	9	):	):	PUNCT
eurjchem-365	128	10	3210	3210	NUM
eurjchem-365	128	11	(nh	(nh	NOUN
eurjchem-365	128	12	)	)	PUNCT
eurjchem-365	128	13	,	,	PUNCT
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eurjchem-365	128	15	(cn	(cn	NOUN
eurjchem-365	128	16	)	)	PUNCT
eurjchem-365	128	17	,	,	PUNCT
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eurjchem-365	128	19	(c	(c	NOUN
eurjchem-365	128	20	=	=	SYM
eurjchem-365	128	21	o	o	NOUN
eurjchem-365	128	22	)	)	PUNCT
eurjchem-365	128	23	(	(	PUNCT
eurjchem-365	128	24	amide	amide	NOUN
eurjchem-365	128	25	)	)	PUNCT
eurjchem-365	128	26	.	.	PUNCT
eurjchem-365	129	1	1h	1h	NUM
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eurjchem-365	129	3	(	(	PUNCT
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eurjchem-365	129	6	,	,	PUNCT
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eurjchem-365	129	8	):	):	PUNCT
eurjchem-365	129	9	7.52‐7.98	7.52‐7.98	NUM
eurjchem-365	129	10	(	(	PUNCT
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eurjchem-365	129	14	,	,	PUNCT
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eurjchem-365	129	16	)	)	PUNCT
eurjchem-365	129	17	,	,	PUNCT
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eurjchem-365	129	19	(	(	PUNCT
eurjchem-365	129	20	s	s	PROPN
eurjchem-365	129	21	,	,	PUNCT
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eurjchem-365	129	23	,	,	PUNCT
eurjchem-365	129	24	=	=	NOUN
eurjchem-365	129	25	ch	ch	NOUN
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eurjchem-365	129	27	,	,	PUNCT
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eurjchem-365	129	36	nh	nh	PROPN
eurjchem-365	129	37	)	)	PUNCT
eurjchem-365	129	38	.	.	PUNCT
eurjchem-365	130	1	ms	ms	NOUN
eurjchem-365	130	2	(	(	PUNCT
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eurjchem-365	130	4	,	,	PUNCT
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eurjchem-365	130	8	):	):	PUNCT
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eurjchem-365	130	10	(	(	PUNCT
eurjchem-365	130	11	m.+	m.+	NOUN
eurjchem-365	130	12	)	)	PUNCT
eurjchem-365	130	13	.	.	PUNCT
eurjchem-365	131	1	anal	anal	PROPN
eurjchem-365	131	2	.	.	PUNCT
eurjchem-365	131	3	calcd	calcd	NOUN
eurjchem-365	131	4	.	.	PUNCT
eurjchem-365	132	1	for	for	ADP
eurjchem-365	132	2	c17h13n3o2	c17h13n3o2	NOUN
eurjchem-365	132	3	:	:	PUNCT
eurjchem-365	132	4	c	c	X
eurjchem-365	132	5	,	,	PUNCT
eurjchem-365	132	6	70.10	70.10	NUM
eurjchem-365	132	7	;	;	PUNCT
eurjchem-365	132	8	h	h	NOUN
eurjchem-365	132	9	,	,	PUNCT
eurjchem-365	132	10	4.46	4.46	NUM
eurjchem-365	132	11	;	;	PUNCT
eurjchem-365	132	12	n	n	CCONJ
eurjchem-365	132	13	,	,	PUNCT
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eurjchem-365	132	15	.	.	PUNCT
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eurjchem-365	132	17	:	:	PUNCT
eurjchem-365	133	1	c	c	X
eurjchem-365	133	2	,	,	PUNCT
eurjchem-365	133	3	69.81	69.81	NUM
eurjchem-365	133	4	;	;	PUNCT
eurjchem-365	133	5	h	h	X
eurjchem-365	133	6	,	,	PUNCT
eurjchem-365	133	7	4.55	4.55	NUM
eurjchem-365	133	8	;	;	PUNCT
eurjchem-365	133	9	n	n	CCONJ
eurjchem-365	133	10	,	,	PUNCT
eurjchem-365	133	11	14.74	14.74	NUM
eurjchem-365	133	12	%	%	NOUN
eurjchem-365	133	13	.	.	PUNCT
eurjchem-365	134	1	2‐n‐(2`‐cyano‐3`‐phenyl‐2`‐propenoyl)aminophenol	2‐n‐(2`‐cyano‐3`‐phenyl‐2`‐propenoyl)aminophenol	NOUN
eurjchem-365	134	2	(	(	PUNCT
eurjchem-365	134	3	20	20	NUM
eurjchem-365	134	4	):	):	PUNCT
eurjchem-365	134	5	compound	compound	NOUN
eurjchem-365	134	6	20	20	NUM
eurjchem-365	134	7	crystallized	crystallize	VERB
eurjchem-365	134	8	from	from	ADP
eurjchem-365	134	9	benzene	benzene	NOUN
eurjchem-365	134	10	to	to	PART
eurjchem-365	134	11	give	give	VERB
eurjchem-365	134	12	yellow	yellow	ADJ
eurjchem-365	134	13	crystals	crystal	NOUN
eurjchem-365	134	14	.	.	PUNCT
eurjchem-365	135	1	yield	yield	NOUN
eurjchem-365	135	2	:	:	PUNCT
eurjchem-365	135	3	50	50	NUM
eurjchem-365	135	4	%	%	NOUN
eurjchem-365	135	5	.	.	PUNCT
eurjchem-365	136	1	m.p	m.p	PROPN
eurjchem-365	136	2	.	.	PROPN
eurjchem-365	136	3	:	:	PUNCT
eurjchem-365	137	1	208‐210	208‐210	NUM
eurjchem-365	137	2	oc	oc	PROPN
eurjchem-365	137	3	.	.	PUNCT
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eurjchem-365	137	5	(	(	PUNCT
eurjchem-365	137	6	kbr	kbr	PROPN
eurjchem-365	137	7	,	,	PUNCT
eurjchem-365	137	8	cm‐1	cm‐1	PROPN
eurjchem-365	137	9	):	):	PUNCT
eurjchem-365	137	10	3368	3368	NUM
eurjchem-365	137	11	,	,	PUNCT
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eurjchem-365	137	13	(oh	(oh	NOUN
eurjchem-365	137	14	)	)	PUNCT
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eurjchem-365	137	17	)	)	PUNCT
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eurjchem-365	137	21	)	)	PUNCT
eurjchem-365	137	22	,	,	PUNCT
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eurjchem-365	137	24	(c	(c	NOUN
eurjchem-365	137	25	=	=	SYM
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eurjchem-365	137	27	)	)	PUNCT
eurjchem-365	137	28	(	(	PUNCT
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eurjchem-365	137	30	)	)	PUNCT
eurjchem-365	137	31	.	.	PUNCT
eurjchem-365	138	1	1h	1h	NUM
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eurjchem-365	138	3	(	(	PUNCT
eurjchem-365	138	4	300	300	NUM
eurjchem-365	138	5	mhz	mhz	NOUN
eurjchem-365	138	6	,	,	PUNCT
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eurjchem-365	138	8	):	):	PUNCT
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eurjchem-365	138	10	,	,	PUNCT
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eurjchem-365	138	14	)	)	PUNCT
eurjchem-365	138	15	,	,	PUNCT
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eurjchem-365	138	17	(	(	PUNCT
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eurjchem-365	138	19	,	,	PUNCT
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eurjchem-365	138	21	,	,	PUNCT
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eurjchem-365	138	25	,	,	PUNCT
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eurjchem-365	138	27	(	(	PUNCT
eurjchem-365	138	28	br	br	PROPN
eurjchem-365	138	29	s	s	PROPN
eurjchem-365	138	30	,	,	PUNCT
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eurjchem-365	138	32	,	,	PUNCT
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eurjchem-365	138	35	,	,	PUNCT
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eurjchem-365	138	39	,	,	PUNCT
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eurjchem-365	138	41	,	,	PUNCT
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eurjchem-365	138	44	.	.	PUNCT
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eurjchem-365	139	4	,	,	PUNCT
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eurjchem-365	139	8	):	):	PUNCT
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eurjchem-365	139	10	(	(	PUNCT
eurjchem-365	139	11	m.+	m.+	NOUN
eurjchem-365	139	12	)	)	PUNCT
eurjchem-365	139	13	.	.	PUNCT
eurjchem-365	140	1	anal	anal	PROPN
eurjchem-365	140	2	.	.	PUNCT
eurjchem-365	140	3	calcd	calcd	NOUN
eurjchem-365	140	4	.	.	PUNCT
eurjchem-365	141	1	for	for	ADP
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eurjchem-365	141	3	:	:	PUNCT
eurjchem-365	141	4	c	c	NOUN
eurjchem-365	141	5	,	,	PUNCT
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eurjchem-365	141	9	,	,	PUNCT
eurjchem-365	141	10	4.54	4.54	NUM
eurjchem-365	141	11	;	;	PUNCT
eurjchem-365	141	12	n	n	CCONJ
eurjchem-365	141	13	,	,	PUNCT
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eurjchem-365	141	17	:	:	PUNCT
eurjchem-365	142	1	c	c	X
eurjchem-365	142	2	,	,	PUNCT
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eurjchem-365	142	5	h	h	X
eurjchem-365	142	6	,	,	PUNCT
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eurjchem-365	142	8	;	;	PUNCT
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eurjchem-365	142	10	,	,	PUNCT
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eurjchem-365	142	13	.	.	PUNCT
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eurjchem-365	143	2	.	.	PUNCT
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eurjchem-365	144	3	(	(	PUNCT
eurjchem-365	144	4	10	10	NUM
eurjchem-365	144	5	)	)	PUNCT
eurjchem-365	144	6	a	a	DET
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eurjchem-365	144	13	(	(	PUNCT
eurjchem-365	144	14	3	3	NUM
eurjchem-365	144	15	g	g	NOUN
eurjchem-365	144	16	)	)	PUNCT
eurjchem-365	144	17	and	and	CCONJ
eurjchem-365	144	18	freshly	freshly	ADV
eurjchem-365	144	19	distilled	distil	VERB
eurjchem-365	144	20	acetic	acetic	ADJ
eurjchem-365	144	21	anhydride	anhydride	NOUN
eurjchem-365	144	22	(	(	PUNCT
eurjchem-365	144	23	10	10	NUM
eurjchem-365	144	24	ml	ml	NOUN
eurjchem-365	144	25	)	)	PUNCT
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eurjchem-365	144	27	heated	heat	VERB
eurjchem-365	144	28	on	on	ADP
eurjchem-365	144	29	water	water	NOUN
eurjchem-365	144	30	bath	bath	NOUN
eurjchem-365	144	31	for	for	ADP
eurjchem-365	144	32	an	an	DET
eurjchem-365	144	33	hour	hour	NOUN
eurjchem-365	144	34	.	.	PUNCT
eurjchem-365	145	1	the	the	DET
eurjchem-365	145	2	solid	solid	ADJ
eurjchem-365	145	3	separated	separate	VERB
eurjchem-365	145	4	out	out	ADP
eurjchem-365	145	5	at	at	ADP
eurjchem-365	145	6	room	room	NOUN
eurjchem-365	145	7	temperature	temperature	NOUN
eurjchem-365	145	8	was	be	AUX
eurjchem-365	145	9	collected	collect	VERB
eurjchem-365	145	10	,	,	PUNCT
eurjchem-365	145	11	washed	wash	VERB
eurjchem-365	145	12	with	with	ADP
eurjchem-365	145	13	dry	dry	ADJ
eurjchem-365	145	14	petroleum	petroleum	NOUN
eurjchem-365	145	15	ether	ether	NOUN
eurjchem-365	145	16	40‐60c	40‐60c	PROPN
eurjchem-365	145	17	,	,	PUNCT
eurjchem-365	145	18	dried	dry	VERB
eurjchem-365	145	19	and	and	CCONJ
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eurjchem-365	145	21	from	from	ADP
eurjchem-365	145	22	light	light	ADJ
eurjchem-365	145	23	petroleum	petroleum	NOUN
eurjchem-365	145	24	(	(	PUNCT
eurjchem-365	145	25	80‐100	80‐100	NOUN
eurjchem-365	145	26	oc	oc	PROPN
eurjchem-365	145	27	)	)	PUNCT
eurjchem-365	145	28	to	to	PART
eurjchem-365	145	29	give	give	VERB
eurjchem-365	145	30	10	10	NUM
eurjchem-365	145	31	as	as	ADP
eurjchem-365	145	32	yellow	yellow	ADJ
eurjchem-365	145	33	crystals	crystal	NOUN
eurjchem-365	145	34	(	(	PUNCT
eurjchem-365	145	35	scheme	scheme	NOUN
eurjchem-365	145	36	1	1	NUM
eurjchem-365	145	37	)	)	PUNCT
eurjchem-365	145	38	.	.	PUNCT
eurjchem-365	146	1	yield	yield	NOUN
eurjchem-365	146	2	:	:	PUNCT
eurjchem-365	146	3	88	88	NUM
eurjchem-365	146	4	%	%	NOUN
eurjchem-365	146	5	.	.	PUNCT
eurjchem-365	147	1	m.p	m.p	PROPN
eurjchem-365	147	2	.	.	PROPN
eurjchem-365	147	3	:	:	PUNCT
eurjchem-365	148	1	190‐192	190‐192	NUM
eurjchem-365	148	2	oc	oc	PROPN
eurjchem-365	148	3	.	.	PROPN
eurjchem-365	148	4	ft‐ir	ft‐ir	NOUN
eurjchem-365	148	5	(	(	PUNCT
eurjchem-365	148	6	kbr	kbr	PROPN
eurjchem-365	148	7	,	,	PUNCT
eurjchem-365	148	8	cm‐1	cm‐1	PROPN
eurjchem-365	148	9	):	):	PUNCT
eurjchem-365	148	10	2227	2227	NUM
eurjchem-365	148	11	(cn	(cn	NOUN
eurjchem-365	148	12	)	)	PUNCT
eurjchem-365	148	13	,	,	PUNCT
eurjchem-365	148	14	1765	1765	NUM
eurjchem-365	148	15	(c	(c	NOUN
eurjchem-365	148	16	=	=	SYM
eurjchem-365	148	17	o	o	NOUN
eurjchem-365	148	18	)	)	PUNCT
eurjchem-365	148	19	(	(	PUNCT
eurjchem-365	148	20	oxazinone	oxazinone	NOUN
eurjchem-365	148	21	)	)	PUNCT
eurjchem-365	148	22	.	.	PUNCT
eurjchem-365	149	1	1h	1h	NUM
eurjchem-365	149	2	nmr	nmr	NOUN
eurjchem-365	149	3	(	(	PUNCT
eurjchem-365	149	4	300	300	NUM
eurjchem-365	149	5	mhz	mhz	NOUN
eurjchem-365	149	6	,	,	PUNCT
eurjchem-365	149	7	dmso‐d6	dmso‐d6	NUM
eurjchem-365	149	8	):	):	PUNCT
eurjchem-365	149	9	7.60‐8.19	7.60‐8.19	NUM
eurjchem-365	149	10	(	(	PUNCT
eurjchem-365	149	11	m	m	PROPN
eurjchem-365	149	12	,	,	PUNCT
eurjchem-365	149	13	9	9	NUM
eurjchem-365	149	14	h	h	NOUN
eurjchem-365	149	15	,	,	PUNCT
eurjchem-365	149	16	ar‐h	ar‐h	NOUN
eurjchem-365	149	17	)	)	PUNCT
eurjchem-365	149	18	,	,	PUNCT
eurjchem-365	149	19	8.46	8.46	NUM
eurjchem-365	149	20	(	(	PUNCT
eurjchem-365	149	21	s	s	PROPN
eurjchem-365	149	22	,	,	PUNCT
eurjchem-365	149	23	1h	1h	NUM
eurjchem-365	149	24	,	,	PUNCT
eurjchem-365	149	25	=	=	NOUN
eurjchem-365	149	26	ch	ch	NOUN
eurjchem-365	149	27	)	)	PUNCT
eurjchem-365	149	28	.	.	PUNCT
eurjchem-365	150	1	ms	ms	NOUN
eurjchem-365	150	2	(	(	PUNCT
eurjchem-365	150	3	ei	ei	PROPN
eurjchem-365	150	4	,	,	PUNCT
eurjchem-365	150	5	m	m	PROPN
eurjchem-365	150	6	/	/	SYM
eurjchem-365	150	7	z	z	NOUN
eurjchem-365	150	8	):	):	PUNCT
eurjchem-365	150	9	274	274	NUM
eurjchem-365	150	10	(	(	PUNCT
eurjchem-365	150	11	m.+	m.+	NOUN
eurjchem-365	150	12	)	)	PUNCT
eurjchem-365	150	13	.	.	PUNCT
eurjchem-365	151	1	anal	anal	PROPN
eurjchem-365	151	2	.	.	PUNCT
eurjchem-365	151	3	calcd	calcd	NOUN
eurjchem-365	151	4	.	.	PUNCT
eurjchem-365	152	1	for	for	ADP
eurjchem-365	152	2	c17h10n2o2	c17h10n2o2	ADJ
eurjchem-365	152	3	:	:	PUNCT
eurjchem-365	152	4	c	c	X
eurjchem-365	152	5	,	,	PUNCT
eurjchem-365	152	6	74.45	74.45	NUM
eurjchem-365	152	7	;	;	PUNCT
eurjchem-365	152	8	h	h	NOUN
eurjchem-365	152	9	,	,	PUNCT
eurjchem-365	152	10	3.64	3.64	NUM
eurjchem-365	152	11	;	;	PUNCT
eurjchem-365	152	12	n	n	CCONJ
eurjchem-365	152	13	,	,	PUNCT
eurjchem-365	152	14	10.21	10.21	NUM
eurjchem-365	152	15	.	.	PUNCT
eurjchem-365	152	16	found	find	VERB
eurjchem-365	152	17	:	:	PUNCT
eurjchem-365	153	1	c	c	X
eurjchem-365	153	2	,	,	PUNCT
eurjchem-365	153	3	74.66	74.66	NUM
eurjchem-365	153	4	;	;	PUNCT
eurjchem-365	153	5	h	h	NOUN
eurjchem-365	153	6	,	,	PUNCT
eurjchem-365	153	7	3.25	3.25	NUM
eurjchem-365	153	8	;	;	PUNCT
eurjchem-365	153	9	n	n	CCONJ
eurjchem-365	153	10	,	,	PUNCT
eurjchem-365	153	11	9.87	9.87	NUM
eurjchem-365	153	12	%	%	NOUN
eurjchem-365	153	13	.	.	PUNCT
eurjchem-365	154	1	2.6	2.6	NUM
eurjchem-365	154	2	.	.	X
eurjchem-365	155	1	2‐(1‐cyano‐2‐phenyl‐ethen‐1‐yl)‐quinazolin‐4(3h)‐one	2‐(1‐cyano‐2‐phenyl‐ethen‐1‐yl)‐quinazolin‐4(3h)‐one	NUM
eurjchem-365	155	2	(	(	PUNCT
eurjchem-365	155	3	11	11	NUM
eurjchem-365	155	4	)	)	PUNCT
eurjchem-365	155	5	a	a	DET
eurjchem-365	155	6	mixture	mixture	NOUN
eurjchem-365	155	7	of	of	ADP
eurjchem-365	155	8	benzoxazinone	benzoxazinone	NOUN
eurjchem-365	155	9	10	10	NUM
eurjchem-365	155	10	(	(	PUNCT
eurjchem-365	155	11	0.9	0.9	NUM
eurjchem-365	155	12	g	g	NOUN
eurjchem-365	155	13	;	;	PUNCT
eurjchem-365	155	14	3	3	NUM
eurjchem-365	155	15	mmol	mmol	NOUN
eurjchem-365	155	16	)	)	PUNCT
eurjchem-365	155	17	and	and	CCONJ
eurjchem-365	155	18	ammonium	ammonium	NOUN
eurjchem-365	155	19	acetate	acetate	NOUN
eurjchem-365	155	20	(	(	PUNCT
eurjchem-365	155	21	1	1	NUM
eurjchem-365	155	22	g	g	NOUN
eurjchem-365	155	23	;	;	PUNCT
eurjchem-365	155	24	12	12	NUM
eurjchem-365	155	25	mmol	mmol	NOUN
eurjchem-365	155	26	)	)	PUNCT
eurjchem-365	155	27	was	be	AUX
eurjchem-365	155	28	heated	heat	VERB
eurjchem-365	155	29	without	without	ADP
eurjchem-365	155	30	solvent	solvent	NOUN
eurjchem-365	155	31	at	at	ADP
eurjchem-365	155	32	160‐170	160‐170	NUM
eurjchem-365	155	33	oc	oc	NOUN
eurjchem-365	155	34	for	for	ADP
eurjchem-365	155	35	four	four	NUM
eurjchem-365	155	36	hours	hour	NOUN
eurjchem-365	155	37	.	.	PUNCT
eurjchem-365	156	1	the	the	DET
eurjchem-365	156	2	solid	solid	ADJ
eurjchem-365	156	3	mass	mass	NOUN
eurjchem-365	156	4	was	be	AUX
eurjchem-365	156	5	triturated	triturate	VERB
eurjchem-365	156	6	with	with	ADP
eurjchem-365	156	7	warm	warm	ADJ
eurjchem-365	156	8	water	water	NOUN
eurjchem-365	156	9	.	.	PUNCT
eurjchem-365	157	1	the	the	DET
eurjchem-365	157	2	solid	solid	ADJ
eurjchem-365	157	3	separated	separate	VERB
eurjchem-365	157	4	was	be	AUX
eurjchem-365	157	5	filtered	filter	VERB
eurjchem-365	157	6	,	,	PUNCT
eurjchem-365	157	7	washed	wash	VERB
eurjchem-365	157	8	with	with	ADP
eurjchem-365	157	9	water	water	NOUN
eurjchem-365	157	10	several	several	ADJ
eurjchem-365	157	11	times	time	NOUN
eurjchem-365	157	12	,	,	PUNCT
eurjchem-365	157	13	dried	dry	VERB
eurjchem-365	157	14	and	and	CCONJ
eurjchem-365	157	15	crystallized	crystallize	VERB
eurjchem-365	157	16	from	from	ADP
eurjchem-365	157	17	dioxane	dioxane	NOUN
eurjchem-365	157	18	to	to	PART
eurjchem-365	157	19	yield	yield	VERB
eurjchem-365	157	20	11	11	NUM
eurjchem-365	157	21	as	as	ADP
eurjchem-365	157	22	yellow	yellow	ADJ
eurjchem-365	157	23	crystals	crystal	NOUN
eurjchem-365	157	24	(	(	PUNCT
eurjchem-365	157	25	scheme	scheme	NOUN
eurjchem-365	157	26	1	1	NUM
eurjchem-365	157	27	)	)	PUNCT
eurjchem-365	157	28	.	.	PUNCT
eurjchem-365	158	1	yield	yield	NOUN
eurjchem-365	158	2	:	:	PUNCT
eurjchem-365	158	3	60	60	NUM
eurjchem-365	158	4	%	%	NOUN
eurjchem-365	158	5	.	.	PUNCT
eurjchem-365	159	1	m.p	m.p	PROPN
eurjchem-365	159	2	.	.	PROPN
eurjchem-365	159	3	:	:	PUNCT
eurjchem-365	160	1	301‐	301‐	NUM
eurjchem-365	160	2	303	303	NUM
eurjchem-365	160	3	oc	oc	NOUN
eurjchem-365	160	4	.	.	PUNCT
eurjchem-365	161	1	ft‐ir	ft‐ir	NOUN
eurjchem-365	161	2	(	(	PUNCT
eurjchem-365	161	3	kbr	kbr	PROPN
eurjchem-365	161	4	,	,	PUNCT
eurjchem-365	161	5	cm‐1	cm‐1	PROPN
eurjchem-365	161	6	):	):	PUNCT
eurjchem-365	161	7	3183	3183	NUM
eurjchem-365	161	8	(nh	(nh	PROPN
eurjchem-365	161	9	)	)	PUNCT
eurjchem-365	161	10	,	,	PUNCT
eurjchem-365	161	11	2228	2228	NUM
eurjchem-365	161	12	(cn	(cn	NOUN
eurjchem-365	161	13	)	)	PUNCT
eurjchem-365	161	14	,	,	PUNCT
eurjchem-365	161	15	1676	1676	NUM
eurjchem-365	161	16	(c	(c	PROPN
eurjchem-365	161	17	=	=	SYM
eurjchem-365	161	18	o	o	NOUN
eurjchem-365	161	19	)	)	PUNCT
eurjchem-365	161	20	(	(	PUNCT
eurjchem-365	161	21	quinazolinone	quinazolinone	NOUN
eurjchem-365	161	22	)	)	PUNCT
eurjchem-365	161	23	.	.	PUNCT
eurjchem-365	162	1	1h	1h	NUM
eurjchem-365	162	2	nmr	nmr	NOUN
eurjchem-365	162	3	(	(	PUNCT
eurjchem-365	162	4	300	300	NUM
eurjchem-365	162	5	mhz	mhz	NOUN
eurjchem-365	162	6	,	,	PUNCT
eurjchem-365	162	7	dmso‐d6	dmso‐d6	NUM
eurjchem-365	162	8	):	):	PUNCT
eurjchem-365	162	9	7.55‐	7.55‐	NUM
eurjchem-365	162	10	8.16	8.16	NUM
eurjchem-365	162	11	(	(	PUNCT
eurjchem-365	162	12	m	m	PROPN
eurjchem-365	162	13	,	,	PUNCT
eurjchem-365	162	14	10	10	NUM
eurjchem-365	162	15	h	h	NOUN
eurjchem-365	162	16	,	,	PUNCT
eurjchem-365	162	17	=	=	NOUN
eurjchem-365	162	18	ch	ch	NOUN
eurjchem-365	162	19	,	,	PUNCT
eurjchem-365	162	20	ar‐h	ar‐h	PROPN
eurjchem-365	162	21	)	)	PUNCT
eurjchem-365	162	22	,	,	PUNCT
eurjchem-365	162	23	8.50	8.50	NUM
eurjchem-365	162	24	(	(	PUNCT
eurjchem-365	162	25	s	s	PROPN
eurjchem-365	162	26	,	,	PUNCT
eurjchem-365	162	27	1h	1h	NUM
eurjchem-365	162	28	,	,	PUNCT
eurjchem-365	162	29	nh	nh	PROPN
eurjchem-365	162	30	)	)	PUNCT
eurjchem-365	162	31	.	.	PUNCT
eurjchem-365	163	1	ms	ms	NOUN
eurjchem-365	163	2	(	(	PUNCT
eurjchem-365	163	3	ei	ei	PROPN
eurjchem-365	163	4	,	,	PUNCT
eurjchem-365	163	5	m	m	PROPN
eurjchem-365	163	6	/	/	SYM
eurjchem-365	163	7	z	z	NOUN
eurjchem-365	163	8	):	):	PUNCT
eurjchem-365	163	9	273	273	NUM
eurjchem-365	163	10	(	(	PUNCT
eurjchem-365	163	11	m.+	m.+	NOUN
eurjchem-365	163	12	)	)	PUNCT
eurjchem-365	163	13	.	.	PUNCT
eurjchem-365	164	1	anal	anal	PROPN
eurjchem-365	164	2	.	.	PUNCT
eurjchem-365	164	3	calcd	calcd	NOUN
eurjchem-365	164	4	.	.	PUNCT
eurjchem-365	165	1	for	for	ADP
eurjchem-365	165	2	c17h11n3o	c17h11n3o	NOUN
eurjchem-365	165	3	:	:	PUNCT
eurjchem-365	165	4	c	c	X
eurjchem-365	165	5	,	,	PUNCT
eurjchem-365	165	6	74.72	74.72	NUM
eurjchem-365	165	7	;	;	PUNCT
eurjchem-365	165	8	h	h	NOUN
eurjchem-365	165	9	,	,	PUNCT
eurjchem-365	165	10	4.02	4.02	NUM
eurjchem-365	165	11	;	;	PUNCT
eurjchem-365	165	12	n	n	CCONJ
eurjchem-365	165	13	,	,	PUNCT
eurjchem-365	165	14	15.38	15.38	NUM
eurjchem-365	165	15	.	.	PUNCT
eurjchem-365	165	16	found	find	VERB
eurjchem-365	165	17	:	:	PUNCT
eurjchem-365	166	1	c	c	X
eurjchem-365	166	2	,	,	PUNCT
eurjchem-365	166	3	75.11	75.11	NUM
eurjchem-365	166	4	;	;	PUNCT
eurjchem-365	166	5	h	h	NOUN
eurjchem-365	166	6	,	,	PUNCT
eurjchem-365	166	7	3.84	3.84	NUM
eurjchem-365	166	8	;	;	PUNCT
eurjchem-365	166	9	n	n	CCONJ
eurjchem-365	166	10	,	,	PUNCT
eurjchem-365	166	11	15.68	15.68	NUM
eurjchem-365	166	12	%	%	NOUN
eurjchem-365	166	13	.	.	PUNCT
eurjchem-365	167	1	2.7	2.7	NUM
eurjchem-365	167	2	.	.	X
eurjchem-365	167	3	2‐(1‐cyano‐2‐phenyl‐ethen‐1‐yl)‐3‐(2‐carboxyphenyl	2‐(1‐cyano‐2‐phenyl‐ethen‐1‐yl)‐3‐(2‐carboxyphenyl	NOUN
eurjchem-365	167	4	)	)	PUNCT
eurjchem-365	167	5	quinazolin‐4‐one	quinazolin‐4‐one	PROPN
eurjchem-365	167	6	(	(	PUNCT
eurjchem-365	167	7	12	12	NUM
eurjchem-365	167	8	)	)	PUNCT
eurjchem-365	167	9	and	and	CCONJ
eurjchem-365	167	10	(	(	PUNCT
eurjchem-365	167	11	e)‐2‐(2‐(2‐cyano‐3‐phenyl	e)‐2‐(2‐(2‐cyano‐3‐phenyl	NOUN
eurjchem-365	167	12	acrylamido)benzamido)benzoic	acrylamido)benzamido)benzoic	X
eurjchem-365	167	13	acid	acid	NOUN
eurjchem-365	167	14	(	(	PUNCT
eurjchem-365	167	15	13	13	NUM
eurjchem-365	167	16	)	)	PUNCT
eurjchem-365	167	17	a	a	DET
eurjchem-365	167	18	mixture	mixture	NOUN
eurjchem-365	167	19	of	of	ADP
eurjchem-365	167	20	1	1	NUM
eurjchem-365	167	21	(	(	PUNCT
eurjchem-365	167	22	1.9	1.9	NUM
eurjchem-365	167	23	g	g	NOUN
eurjchem-365	167	24	;	;	PUNCT
eurjchem-365	167	25	10	10	NUM
eurjchem-365	167	26	mmol	mmol	NOUN
eurjchem-365	167	27	)	)	PUNCT
eurjchem-365	167	28	and	and	CCONJ
eurjchem-365	167	29	anthranilic	anthranilic	NOUN
eurjchem-365	167	30	acid	acid	NOUN
eurjchem-365	167	31	(	(	PUNCT
eurjchem-365	167	32	1.36	1.36	NUM
eurjchem-365	167	33	g	g	NOUN
eurjchem-365	167	34	,	,	PUNCT
eurjchem-365	167	35	10	10	NUM
eurjchem-365	167	36	mmol	mmol	NOUN
eurjchem-365	167	37	)	)	PUNCT
eurjchem-365	167	38	in	in	ADP
eurjchem-365	167	39	dry	dry	ADJ
eurjchem-365	167	40	pyridine	pyridine	NOUN
eurjchem-365	167	41	(	(	PUNCT
eurjchem-365	167	42	30	30	NUM
eurjchem-365	167	43	ml	ml	NOUN
eurjchem-365	167	44	)	)	PUNCT
eurjchem-365	167	45	was	be	AUX
eurjchem-365	167	46	refluxed	refluxe	VERB
eurjchem-365	167	47	for	for	ADP
eurjchem-365	167	48	two	two	NUM
eurjchem-365	167	49	hours	hour	NOUN
eurjchem-365	167	50	.	.	PUNCT
eurjchem-365	168	1	after	after	ADP
eurjchem-365	168	2	cooling	cool	VERB
eurjchem-365	168	3	the	the	DET
eurjchem-365	168	4	mixture	mixture	NOUN
eurjchem-365	168	5	was	be	AUX
eurjchem-365	168	6	acidified	acidify	VERB
eurjchem-365	168	7	with	with	ADP
eurjchem-365	168	8	cold	cold	ADJ
eurjchem-365	168	9	dilute	dilute	NOUN
eurjchem-365	168	10	hcl	hcl	PROPN
eurjchem-365	168	11	.	.	PUNCT
eurjchem-365	169	1	the	the	DET
eurjchem-365	169	2	shiba	shiba	PROPN
eurjchem-365	169	3	et	et	PROPN
eurjchem-365	169	4	al	al	PROPN
eurjchem-365	169	5	.	.	PUNCT
eurjchem-365	169	6	/	/	SYM
eurjchem-365	169	7	european	european	PROPN
eurjchem-365	169	8	journal	journal	PROPN
eurjchem-365	169	9	of	of	ADP
eurjchem-365	169	10	chemistry	chemistry	NOUN
eurjchem-365	169	11	2	2	NUM
eurjchem-365	169	12	(	(	PUNCT
eurjchem-365	169	13	2	2	NUM
eurjchem-365	169	14	)	)	PUNCT
eurjchem-365	169	15	(	(	PUNCT
eurjchem-365	169	16	2011	2011	NUM
eurjchem-365	169	17	)	)	PUNCT
eurjchem-365	169	18	200‐205	200‐205	NUM
eurjchem-365	169	19	203	203	NUM
eurjchem-365	169	20	precipitate	precipitate	NOUN
eurjchem-365	169	21	formed	form	VERB
eurjchem-365	169	22	was	be	AUX
eurjchem-365	169	23	collected	collect	VERB
eurjchem-365	169	24	,	,	PUNCT
eurjchem-365	169	25	washed	wash	VERB
eurjchem-365	169	26	with	with	ADP
eurjchem-365	169	27	water	water	NOUN
eurjchem-365	169	28	,	,	PUNCT
eurjchem-365	169	29	dried	dry	VERB
eurjchem-365	169	30	and	and	CCONJ
eurjchem-365	169	31	triturated	triturate	VERB
eurjchem-365	169	32	by	by	ADP
eurjchem-365	169	33	ethanol	ethanol	NOUN
eurjchem-365	169	34	then	then	ADV
eurjchem-365	169	35	fractionally	fractionally	ADV
eurjchem-365	169	36	crystallized	crystallize	VERB
eurjchem-365	169	37	to	to	PART
eurjchem-365	169	38	afford	afford	VERB
eurjchem-365	169	39	quinazolinone	quinazolinone	PROPN
eurjchem-365	169	40	12	12	NUM
eurjchem-365	169	41	and	and	CCONJ
eurjchem-365	169	42	benzamide	benzamide	VERB
eurjchem-365	169	43	derivative	derivative	ADJ
eurjchem-365	169	44	13	13	NUM
eurjchem-365	169	45	(	(	PUNCT
eurjchem-365	169	46	scheme	scheme	NOUN
eurjchem-365	169	47	1	1	NUM
eurjchem-365	169	48	)	)	PUNCT
eurjchem-365	169	49	.	.	PUNCT
eurjchem-365	170	1	compound	compound	NOUN
eurjchem-365	170	2	12	12	NUM
eurjchem-365	170	3	crystallized	crystallize	VERB
eurjchem-365	170	4	from	from	ADP
eurjchem-365	170	5	light	light	ADJ
eurjchem-365	170	6	petroleum	petroleum	NOUN
eurjchem-365	170	7	(	(	PUNCT
eurjchem-365	170	8	80‐100	80‐100	NOUN
eurjchem-365	170	9	oc	oc	PROPN
eurjchem-365	170	10	)	)	PUNCT
eurjchem-365	170	11	to	to	PART
eurjchem-365	170	12	give	give	VERB
eurjchem-365	170	13	yellow	yellow	ADJ
eurjchem-365	170	14	crystals	crystal	NOUN
eurjchem-365	170	15	.	.	PUNCT
eurjchem-365	171	1	yield	yield	NOUN
eurjchem-365	171	2	:	:	PUNCT
eurjchem-365	171	3	65	65	NUM
eurjchem-365	171	4	%	%	NOUN
eurjchem-365	171	5	.	.	PUNCT
eurjchem-365	172	1	m.p	m.p	PROPN
eurjchem-365	172	2	.	.	PROPN
eurjchem-365	172	3	:	:	PUNCT
eurjchem-365	173	1	190‐192	190‐192	NUM
eurjchem-365	173	2	oc	oc	PROPN
eurjchem-365	173	3	.	.	PROPN
eurjchem-365	173	4	ft‐ir	ft‐ir	NOUN
eurjchem-365	173	5	(	(	PUNCT
eurjchem-365	173	6	kbr	kbr	PROPN
eurjchem-365	173	7	,	,	PUNCT
eurjchem-365	173	8	cm‐1	cm‐1	PROPN
eurjchem-365	173	9	):	):	PUNCT
eurjchem-365	173	10	3750	3750	NUM
eurjchem-365	173	11	,	,	PUNCT
eurjchem-365	173	12	3315	3315	NUM
eurjchem-365	173	13	(oh	(oh	NOUN
eurjchem-365	173	14	)	)	PUNCT
eurjchem-365	173	15	and	and	CCONJ
eurjchem-365	173	16	(nh	(nh	NOUN
eurjchem-365	173	17	)	)	PUNCT
eurjchem-365	173	18	,	,	PUNCT
eurjchem-365	173	19	2213	2213	NUM
eurjchem-365	173	20	(cn	(cn	NOUN
eurjchem-365	173	21	)	)	PUNCT
eurjchem-365	173	22	,	,	PUNCT
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eurjchem-365	173	24	(c	(c	PROPN
eurjchem-365	173	25	=	=	SYM
eurjchem-365	173	26	o	o	NOUN
eurjchem-365	173	27	)	)	PUNCT
eurjchem-365	173	28	(	(	PUNCT
eurjchem-365	173	29	acid	acid	NOUN
eurjchem-365	173	30	)	)	PUNCT
eurjchem-365	173	31	,	,	PUNCT
eurjchem-365	173	32	1660	1660	NUM
eurjchem-365	173	33	(c	(c	PROPN
eurjchem-365	173	34	=	=	SYM
eurjchem-365	173	35	o	o	NOUN
eurjchem-365	173	36	)	)	PUNCT
eurjchem-365	173	37	(	(	PUNCT
eurjchem-365	173	38	cyclic	cyclic	ADJ
eurjchem-365	173	39	amide	amide	NOUN
eurjchem-365	173	40	)	)	PUNCT
eurjchem-365	173	41	.	.	PUNCT
eurjchem-365	174	1	1h	1h	NUM
eurjchem-365	174	2	nmr	nmr	NOUN
eurjchem-365	174	3	(	(	PUNCT
eurjchem-365	174	4	300	300	NUM
eurjchem-365	174	5	mhz	mhz	NOUN
eurjchem-365	174	6	,	,	PUNCT
eurjchem-365	174	7	dmso‐d6	dmso‐d6	NUM
eurjchem-365	174	8	):	):	PUNCT
eurjchem-365	174	9	7.24‐8.59	7.24‐8.59	NUM
eurjchem-365	174	10	(	(	PUNCT
eurjchem-365	174	11	m	m	PROPN
eurjchem-365	174	12	,	,	PUNCT
eurjchem-365	174	13	14	14	NUM
eurjchem-365	174	14	h	h	NOUN
eurjchem-365	174	15	,	,	PUNCT
eurjchem-365	174	16	=	=	NOUN
eurjchem-365	174	17	ch	ch	NOUN
eurjchem-365	174	18	,	,	PUNCT
eurjchem-365	174	19	ar‐h	ar‐h	PROPN
eurjchem-365	174	20	)	)	PUNCT
eurjchem-365	174	21	,	,	PUNCT
eurjchem-365	174	22	12.09	12.09	NUM
eurjchem-365	174	23	(	(	PUNCT
eurjchem-365	174	24	s	s	PROPN
eurjchem-365	174	25	,	,	PUNCT
eurjchem-365	174	26	1h	1h	NUM
eurjchem-365	174	27	,	,	PUNCT
eurjchem-365	174	28	oh	oh	INTJ
eurjchem-365	174	29	)	)	PUNCT
eurjchem-365	174	30	.	.	PUNCT
eurjchem-365	175	1	ms	ms	NOUN
eurjchem-365	175	2	(	(	PUNCT
eurjchem-365	175	3	ei	ei	PROPN
eurjchem-365	175	4	,	,	PUNCT
eurjchem-365	175	5	m	m	PROPN
eurjchem-365	175	6	/	/	SYM
eurjchem-365	175	7	z	z	NOUN
eurjchem-365	175	8	):	):	PUNCT
eurjchem-365	175	9	393	393	NUM
eurjchem-365	175	10	(	(	PUNCT
eurjchem-365	175	11	m.+	m.+	NOUN
eurjchem-365	175	12	)	)	PUNCT
eurjchem-365	175	13	.	.	PUNCT
eurjchem-365	176	1	anal	anal	PROPN
eurjchem-365	176	2	.	.	PUNCT
eurjchem-365	176	3	calcd	calcd	NOUN
eurjchem-365	176	4	.	.	PUNCT
eurjchem-365	177	1	for	for	ADP
eurjchem-365	177	2	c24h15n3o3	c24h15n3o3	NOUN
eurjchem-365	177	3	:	:	PUNCT
eurjchem-365	177	4	c	c	X
eurjchem-365	177	5	,	,	PUNCT
eurjchem-365	177	6	73.28	73.28	NUM
eurjchem-365	177	7	;	;	PUNCT
eurjchem-365	177	8	h	h	NOUN
eurjchem-365	177	9	,	,	PUNCT
eurjchem-365	177	10	3.84	3.84	NUM
eurjchem-365	177	11	;	;	PUNCT
eurjchem-365	177	12	n	n	CCONJ
eurjchem-365	177	13	,	,	PUNCT
eurjchem-365	177	14	10.68	10.68	NUM
eurjchem-365	177	15	.	.	PUNCT
eurjchem-365	177	16	found	find	VERB
eurjchem-365	177	17	:	:	PUNCT
eurjchem-365	178	1	c	c	X
eurjchem-365	178	2	,	,	PUNCT
eurjchem-365	178	3	73.01	73.01	NUM
eurjchem-365	178	4	;	;	PUNCT
eurjchem-365	178	5	h	h	NOUN
eurjchem-365	178	6	,	,	PUNCT
eurjchem-365	178	7	4.00	4.00	NUM
eurjchem-365	178	8	;	;	PUNCT
eurjchem-365	178	9	n	n	CCONJ
eurjchem-365	178	10	,	,	PUNCT
eurjchem-365	178	11	10.90	10.90	NUM
eurjchem-365	178	12	%	%	NOUN
eurjchem-365	178	13	.	.	PUNCT
eurjchem-365	179	1	compound	compound	NOUN
eurjchem-365	179	2	13	13	NUM
eurjchem-365	179	3	crystallized	crystallize	VERB
eurjchem-365	179	4	from	from	ADP
eurjchem-365	179	5	benzene	benzene	NOUN
eurjchem-365	179	6	/	/	SYM
eurjchem-365	179	7	ethanol	ethanol	NOUN
eurjchem-365	179	8	to	to	PART
eurjchem-365	179	9	give	give	VERB
eurjchem-365	179	10	brown	brown	ADJ
eurjchem-365	179	11	crystals	crystal	NOUN
eurjchem-365	179	12	.	.	PUNCT
eurjchem-365	180	1	yield	yield	NOUN
eurjchem-365	180	2	:	:	PUNCT
eurjchem-365	180	3	15	15	NUM
eurjchem-365	180	4	%	%	NOUN
eurjchem-365	180	5	.	.	PUNCT
eurjchem-365	181	1	m.p	m.p	PROPN
eurjchem-365	181	2	.	.	PROPN
eurjchem-365	181	3	:	:	PUNCT
eurjchem-365	182	1	220‐223	220‐223	NUM
eurjchem-365	182	2	oc	oc	PROPN
eurjchem-365	182	3	.	.	PUNCT
eurjchem-365	182	4	ft‐ir	ft‐ir	NOUN
eurjchem-365	182	5	(	(	PUNCT
eurjchem-365	182	6	kbr	kbr	PROPN
eurjchem-365	182	7	,	,	PUNCT
eurjchem-365	182	8	cm‐1	cm‐1	PROPN
eurjchem-365	182	9	):	):	PUNCT
eurjchem-365	182	10	3340	3340	NUM
eurjchem-365	182	11	,	,	PUNCT
eurjchem-365	182	12	2640	2640	NUM
eurjchem-365	182	13	(oh	(oh	NOUN
eurjchem-365	182	14	)	)	PUNCT
eurjchem-365	182	15	and	and	CCONJ
eurjchem-365	182	16	(nh	(nh	NOUN
eurjchem-365	182	17	)	)	PUNCT
eurjchem-365	182	18	,	,	PUNCT
eurjchem-365	182	19	2210	2210	NUM
eurjchem-365	182	20	(cn	(cn	NOUN
eurjchem-365	182	21	)	)	PUNCT
eurjchem-365	182	22	,	,	PUNCT
eurjchem-365	182	23	1681	1681	NUM
eurjchem-365	182	24	(c	(c	PROPN
eurjchem-365	182	25	=	=	SYM
eurjchem-365	182	26	o	o	NOUN
eurjchem-365	182	27	)	)	PUNCT
eurjchem-365	182	28	.	.	PUNCT
eurjchem-365	183	1	1h	1h	NUM
eurjchem-365	183	2	nmr	nmr	NOUN
eurjchem-365	183	3	(	(	PUNCT
eurjchem-365	183	4	300	300	NUM
eurjchem-365	183	5	mhz	mhz	NOUN
eurjchem-365	183	6	,	,	PUNCT
eurjchem-365	183	7	dmso‐d6	dmso‐d6	NUM
eurjchem-365	183	8	):	):	PUNCT
eurjchem-365	183	9	7.22	7.22	NUM
eurjchem-365	183	10	‐8.62	‐8.62	NUM
eurjchem-365	183	11	(	(	PUNCT
eurjchem-365	183	12	m	m	PROPN
eurjchem-365	183	13	,	,	PUNCT
eurjchem-365	183	14	14h	14h	NUM
eurjchem-365	183	15	,	,	PUNCT
eurjchem-365	183	16	=	=	NOUN
eurjchem-365	183	17	ch	ch	NOUN
eurjchem-365	183	18	,	,	PUNCT
eurjchem-365	183	19	ar‐h	ar‐h	PROPN
eurjchem-365	183	20	)	)	PUNCT
eurjchem-365	183	21	,	,	PUNCT
eurjchem-365	183	22	11.63	11.63	NUM
eurjchem-365	183	23	(	(	PUNCT
eurjchem-365	183	24	s	s	PROPN
eurjchem-365	183	25	,	,	PUNCT
eurjchem-365	183	26	1h	1h	NUM
eurjchem-365	183	27	,	,	PUNCT
eurjchem-365	183	28	nh	nh	PROPN
eurjchem-365	183	29	)	)	PUNCT
eurjchem-365	183	30	,	,	PUNCT
eurjchem-365	183	31	12.07	12.07	NUM
eurjchem-365	183	32	(	(	PUNCT
eurjchem-365	183	33	s	s	PROPN
eurjchem-365	183	34	,	,	PUNCT
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eurjchem-365	183	36	,	,	PUNCT
eurjchem-365	183	37	nh	nh	PROPN
eurjchem-365	183	38	)	)	PUNCT
eurjchem-365	183	39	,	,	PUNCT
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eurjchem-365	183	41	(	(	PUNCT
eurjchem-365	183	42	s	s	PROPN
eurjchem-365	183	43	,	,	PUNCT
eurjchem-365	183	44	1h	1h	NUM
eurjchem-365	183	45	,	,	PUNCT
eurjchem-365	183	46	cooh	cooh	NOUN
eurjchem-365	183	47	)	)	PUNCT
eurjchem-365	183	48	.	.	PUNCT
eurjchem-365	184	1	ms	ms	NOUN
eurjchem-365	184	2	(	(	PUNCT
eurjchem-365	184	3	ei	ei	PROPN
eurjchem-365	184	4	,	,	PUNCT
eurjchem-365	184	5	m	m	PROPN
eurjchem-365	184	6	/	/	SYM
eurjchem-365	184	7	z	z	NOUN
eurjchem-365	184	8	):	):	PUNCT
eurjchem-365	184	9	411	411	NUM
eurjchem-365	184	10	(	(	PUNCT
eurjchem-365	184	11	m.+	m.+	NOUN
eurjchem-365	184	12	)	)	PUNCT
eurjchem-365	184	13	.	.	PUNCT
eurjchem-365	185	1	anal	anal	PROPN
eurjchem-365	185	2	.	.	PUNCT
eurjchem-365	185	3	calcd	calcd	NOUN
eurjchem-365	185	4	.	.	PUNCT
eurjchem-365	186	1	for	for	ADP
eurjchem-365	186	2	c24h17n3o4	c24h17n3o4	PROPN
eurjchem-365	186	3	:	:	PUNCT
eurjchem-365	186	4	c	c	X
eurjchem-365	186	5	,	,	PUNCT
eurjchem-365	186	6	70.07	70.07	NUM
eurjchem-365	186	7	;	;	PUNCT
eurjchem-365	186	8	h	h	NOUN
eurjchem-365	186	9	,	,	PUNCT
eurjchem-365	186	10	4.17	4.17	NUM
eurjchem-365	186	11	;	;	PUNCT
eurjchem-365	186	12	n	n	CCONJ
eurjchem-365	186	13	,	,	PUNCT
eurjchem-365	186	14	10.21	10.21	NUM
eurjchem-365	186	15	.	.	PUNCT
eurjchem-365	186	16	found	find	VERB
eurjchem-365	186	17	:	:	PUNCT
eurjchem-365	187	1	c	c	X
eurjchem-365	187	2	,	,	PUNCT
eurjchem-365	187	3	70.31	70.31	NUM
eurjchem-365	187	4	;	;	PUNCT
eurjchem-365	187	5	h	h	NOUN
eurjchem-365	187	6	,	,	PUNCT
eurjchem-365	187	7	3.92	3.92	NUM
eurjchem-365	187	8	;	;	PUNCT
eurjchem-365	187	9	n	n	CCONJ
eurjchem-365	187	10	,	,	PUNCT
eurjchem-365	187	11	10.00	10.00	NUM
eurjchem-365	187	12	%	%	NOUN
eurjchem-365	187	13	.	.	PUNCT
eurjchem-365	188	1	2.8	2.8	NUM
eurjchem-365	188	2	.	.	PUNCT
eurjchem-365	188	3	conversion	conversion	NOUN
eurjchem-365	188	4	of	of	ADP
eurjchem-365	188	5	benzoxazinone	benzoxazinone	NOUN
eurjchem-365	188	6	(	(	PUNCT
eurjchem-365	188	7	10	10	NUM
eurjchem-365	188	8	)	)	PUNCT
eurjchem-365	188	9	into	into	ADP
eurjchem-365	188	10	(	(	PUNCT
eurjchem-365	188	11	12	12	NUM
eurjchem-365	188	12	)	)	PUNCT
eurjchem-365	188	13	and	and	CCONJ
eurjchem-365	188	14	(	(	PUNCT
eurjchem-365	188	15	13	13	NUM
eurjchem-365	188	16	)	)	PUNCT
eurjchem-365	188	17	procedure	procedure	NOUN
eurjchem-365	188	18	(	(	PUNCT
eurjchem-365	188	19	i	i	NOUN
eurjchem-365	188	20	)	)	PUNCT
eurjchem-365	188	21	in	in	ADP
eurjchem-365	188	22	ethanol	ethanol	NOUN
eurjchem-365	188	23	:	:	PUNCT
eurjchem-365	188	24	a	a	DET
eurjchem-365	188	25	mixture	mixture	NOUN
eurjchem-365	188	26	of	of	ADP
eurjchem-365	188	27	benzoxazinone	benzoxazinone	NOUN
eurjchem-365	188	28	10	10	NUM
eurjchem-365	188	29	(	(	PUNCT
eurjchem-365	188	30	1.49	1.49	NUM
eurjchem-365	188	31	g	g	NOUN
eurjchem-365	188	32	;	;	PUNCT
eurjchem-365	188	33	5	5	NUM
eurjchem-365	188	34	mmol	mmol	NOUN
eurjchem-365	188	35	)	)	PUNCT
eurjchem-365	188	36	and	and	CCONJ
eurjchem-365	188	37	anthranilic	anthranilic	NOUN
eurjchem-365	188	38	acid	acid	NOUN
eurjchem-365	188	39	(	(	PUNCT
eurjchem-365	188	40	0.9	0.9	NUM
eurjchem-365	188	41	g	g	NOUN
eurjchem-365	188	42	;	;	PUNCT
eurjchem-365	188	43	5	5	NUM
eurjchem-365	188	44	mmol	mmol	NOUN
eurjchem-365	188	45	)	)	PUNCT
eurjchem-365	188	46	in	in	ADP
eurjchem-365	188	47	ethanol	ethanol	NOUN
eurjchem-365	188	48	(	(	PUNCT
eurjchem-365	188	49	50	50	NUM
eurjchem-365	188	50	ml	ml	NOUN
eurjchem-365	188	51	)	)	PUNCT
eurjchem-365	188	52	was	be	AUX
eurjchem-365	188	53	refluxed	refluxe	VERB
eurjchem-365	188	54	for	for	ADP
eurjchem-365	188	55	3	3	NUM
eurjchem-365	188	56	h.	h.	NOUN
eurjchem-365	188	57	the	the	DET
eurjchem-365	188	58	solvent	solvent	NOUN
eurjchem-365	188	59	was	be	AUX
eurjchem-365	188	60	distilled	distil	VERB
eurjchem-365	188	61	off	off	ADP
eurjchem-365	188	62	and	and	CCONJ
eurjchem-365	188	63	the	the	DET
eurjchem-365	188	64	residue	residue	NOUN
eurjchem-365	188	65	was	be	AUX
eurjchem-365	188	66	fractionally	fractionally	ADV
eurjchem-365	188	67	crystallized	crystallize	VERB
eurjchem-365	188	68	to	to	PART
eurjchem-365	188	69	give	give	VERB
eurjchem-365	188	70	12	12	NUM
eurjchem-365	188	71	in	in	ADP
eurjchem-365	188	72	10	10	NUM
eurjchem-365	188	73	%	%	NOUN
eurjchem-365	188	74	yield	yield	NOUN
eurjchem-365	188	75	and	and	CCONJ
eurjchem-365	188	76	13	13	NUM
eurjchem-365	188	77	in	in	ADP
eurjchem-365	188	78	90	90	NUM
eurjchem-365	188	79	%	%	NOUN
eurjchem-365	188	80	yield	yield	NOUN
eurjchem-365	188	81	(	(	PUNCT
eurjchem-365	188	82	scheme	scheme	NOUN
eurjchem-365	188	83	1	1	NUM
eurjchem-365	188	84	)	)	PUNCT
eurjchem-365	188	85	.	.	PUNCT
eurjchem-365	189	1	procedure	procedure	NOUN
eurjchem-365	189	2	(	(	PUNCT
eurjchem-365	189	3	ii	ii	NOUN
eurjchem-365	189	4	)	)	PUNCT
eurjchem-365	189	5	heating	heating	NOUN
eurjchem-365	189	6	without	without	ADP
eurjchem-365	189	7	solvent	solvent	NOUN
eurjchem-365	189	8	:	:	PUNCT
eurjchem-365	189	9	the	the	DET
eurjchem-365	189	10	same	same	ADJ
eurjchem-365	189	11	previous	previous	ADJ
eurjchem-365	189	12	mixture	mixture	NOUN
eurjchem-365	189	13	was	be	AUX
eurjchem-365	189	14	heated	heat	VERB
eurjchem-365	189	15	at	at	ADP
eurjchem-365	189	16	140‐160	140‐160	NUM
eurjchem-365	189	17	oc	oc	NOUN
eurjchem-365	189	18	without	without	ADP
eurjchem-365	189	19	solvent	solvent	NOUN
eurjchem-365	189	20	for	for	ADP
eurjchem-365	189	21	1	1	NUM
eurjchem-365	189	22	h.	h.	NOUN
eurjchem-365	189	23	after	after	ADP
eurjchem-365	189	24	cooling	cool	VERB
eurjchem-365	189	25	,	,	PUNCT
eurjchem-365	189	26	the	the	DET
eurjchem-365	189	27	residue	residue	NOUN
eurjchem-365	189	28	was	be	AUX
eurjchem-365	189	29	fractionally	fractionally	ADV
eurjchem-365	189	30	crystallized	crystallize	VERB
eurjchem-365	189	31	to	to	PART
eurjchem-365	189	32	give	give	VERB
eurjchem-365	189	33	12	12	NUM
eurjchem-365	189	34	and	and	CCONJ
eurjchem-365	189	35	13	13	NUM
eurjchem-365	189	36	in	in	ADP
eurjchem-365	189	37	80	80	NUM
eurjchem-365	189	38	%	%	NOUN
eurjchem-365	189	39	and	and	CCONJ
eurjchem-365	189	40	20	20	NUM
eurjchem-365	189	41	%	%	NOUN
eurjchem-365	189	42	yield	yield	NOUN
eurjchem-365	189	43	,	,	PUNCT
eurjchem-365	189	44	respectively	respectively	ADV
eurjchem-365	189	45	(	(	PUNCT
eurjchem-365	189	46	scheme	scheme	NOUN
eurjchem-365	189	47	1	1	NUM
eurjchem-365	189	48	)	)	PUNCT
eurjchem-365	189	49	.	.	PUNCT
eurjchem-365	190	1	2.9	2.9	NUM
eurjchem-365	190	2	.	.	PUNCT
eurjchem-365	191	1	2‐[2‐n‐(2‐cyano‐3‐phenyl‐2‐propenoyl)amino]phenyl‐	2‐[2‐n‐(2‐cyano‐3‐phenyl‐2‐propenoyl)amino]phenyl‐	NUM
eurjchem-365	191	2	4h‐benzo[d][1,3]oxazin‐4‐one	4h‐benzo[d][1,3]oxazin‐4‐one	NOUN
eurjchem-365	191	3	(	(	PUNCT
eurjchem-365	191	4	14	14	NUM
eurjchem-365	191	5	)	)	PUNCT
eurjchem-365	191	6	,	,	PUNCT
eurjchem-365	191	7	(	(	PUNCT
eurjchem-365	191	8	10	10	NUM
eurjchem-365	191	9	)	)	PUNCT
eurjchem-365	191	10	and	and	CCONJ
eurjchem-365	191	11	(	(	PUNCT
eurjchem-365	191	12	12	12	NUM
eurjchem-365	191	13	)	)	PUNCT
eurjchem-365	191	14	a	a	DET
eurjchem-365	191	15	mixture	mixture	NOUN
eurjchem-365	191	16	of	of	ADP
eurjchem-365	191	17	benzamide	benzamide	NOUN
eurjchem-365	191	18	derivative	derivative	NOUN
eurjchem-365	191	19	(	(	PUNCT
eurjchem-365	191	20	13	13	NUM
eurjchem-365	191	21	)	)	PUNCT
eurjchem-365	191	22	(	(	PUNCT
eurjchem-365	191	23	2	2	NUM
eurjchem-365	191	24	g	g	NOUN
eurjchem-365	191	25	)	)	PUNCT
eurjchem-365	191	26	and	and	CCONJ
eurjchem-365	191	27	acetic	acetic	ADJ
eurjchem-365	191	28	anhydride	anhydride	NOUN
eurjchem-365	191	29	(	(	PUNCT
eurjchem-365	191	30	30	30	NUM
eurjchem-365	191	31	ml	ml	NOUN
eurjchem-365	191	32	)	)	PUNCT
eurjchem-365	191	33	was	be	AUX
eurjchem-365	191	34	heated	heat	VERB
eurjchem-365	191	35	on	on	ADP
eurjchem-365	191	36	water	water	NOUN
eurjchem-365	191	37	bath	bath	NOUN
eurjchem-365	191	38	for	for	ADP
eurjchem-365	191	39	two	two	NUM
eurjchem-365	191	40	hours	hour	NOUN
eurjchem-365	191	41	,	,	PUNCT
eurjchem-365	191	42	and	and	CCONJ
eurjchem-365	191	43	then	then	ADV
eurjchem-365	191	44	poured	pour	VERB
eurjchem-365	191	45	into	into	ADP
eurjchem-365	191	46	crushed	crush	VERB
eurjchem-365	191	47	ice	ice	NOUN
eurjchem-365	191	48	.	.	PUNCT
eurjchem-365	192	1	the	the	DET
eurjchem-365	192	2	solid	solid	ADJ
eurjchem-365	192	3	separated	separate	VERB
eurjchem-365	192	4	was	be	AUX
eurjchem-365	192	5	collected	collect	VERB
eurjchem-365	192	6	,	,	PUNCT
eurjchem-365	192	7	washed	wash	VERB
eurjchem-365	192	8	with	with	ADP
eurjchem-365	192	9	water	water	NOUN
eurjchem-365	192	10	,	,	PUNCT
eurjchem-365	192	11	dried	dry	VERB
eurjchem-365	192	12	and	and	CCONJ
eurjchem-365	192	13	fractionally	fractionally	ADV
eurjchem-365	192	14	crystallized	crystallize	VERB
eurjchem-365	192	15	to	to	PART
eurjchem-365	192	16	give	give	VERB
eurjchem-365	192	17	a	a	DET
eurjchem-365	192	18	mixture	mixture	NOUN
eurjchem-365	192	19	of	of	ADP
eurjchem-365	192	20	10	10	NUM
eurjchem-365	192	21	,	,	PUNCT
eurjchem-365	192	22	12	12	NUM
eurjchem-365	192	23	and	and	CCONJ
eurjchem-365	192	24	14	14	NUM
eurjchem-365	192	25	in	in	ADP
eurjchem-365	192	26	5	5	NUM
eurjchem-365	192	27	,	,	PUNCT
eurjchem-365	192	28	25	25	NUM
eurjchem-365	192	29	,	,	PUNCT
eurjchem-365	192	30	45	45	NUM
eurjchem-365	192	31	%	%	NOUN
eurjchem-365	192	32	yields	yield	NOUN
eurjchem-365	192	33	,	,	PUNCT
eurjchem-365	192	34	respectively	respectively	ADV
eurjchem-365	192	35	(	(	PUNCT
eurjchem-365	192	36	scheme	scheme	NOUN
eurjchem-365	192	37	1	1	NUM
eurjchem-365	192	38	)	)	PUNCT
eurjchem-365	192	39	.	.	PUNCT
eurjchem-365	193	1	compound	compound	NOUN
eurjchem-365	193	2	14	14	NUM
eurjchem-365	193	3	was	be	AUX
eurjchem-365	193	4	crystallized	crystallize	VERB
eurjchem-365	193	5	from	from	ADP
eurjchem-365	193	6	dioxane	dioxane	NOUN
eurjchem-365	193	7	to	to	PART
eurjchem-365	193	8	give	give	VERB
eurjchem-365	193	9	pale	pale	ADJ
eurjchem-365	193	10	yellow	yellow	ADJ
eurjchem-365	193	11	crystals	crystal	NOUN
eurjchem-365	193	12	.	.	PUNCT
eurjchem-365	194	1	yield	yield	NOUN
eurjchem-365	194	2	:	:	PUNCT
eurjchem-365	194	3	45	45	NUM
eurjchem-365	194	4	%	%	NOUN
eurjchem-365	194	5	.	.	PUNCT
eurjchem-365	195	1	m.p	m.p	PROPN
eurjchem-365	195	2	.	.	PROPN
eurjchem-365	195	3	:	:	PUNCT
eurjchem-365	196	1	271‐274	271‐274	NUM
eurjchem-365	196	2	oc	oc	NOUN
eurjchem-365	196	3	.	.	PUNCT
eurjchem-365	196	4	ft‐ir	ft‐ir	NOUN
eurjchem-365	196	5	(	(	PUNCT
eurjchem-365	196	6	kbr	kbr	PROPN
eurjchem-365	196	7	,	,	PUNCT
eurjchem-365	196	8	cm‐1	cm‐1	PROPN
eurjchem-365	196	9	):	):	PUNCT
eurjchem-365	196	10	3172	3172	NUM
eurjchem-365	196	11	(nh	(nh	PROPN
eurjchem-365	196	12	)	)	PUNCT
eurjchem-365	196	13	,	,	PUNCT
eurjchem-365	196	14	2208	2208	NUM
eurjchem-365	196	15	(cn	(cn	NOUN
eurjchem-365	196	16	)	)	PUNCT
eurjchem-365	196	17	,	,	PUNCT
eurjchem-365	196	18	1763	1763	NUM
eurjchem-365	196	19	(c	(c	PROPN
eurjchem-365	196	20	=	=	SYM
eurjchem-365	196	21	o	o	NOUN
eurjchem-365	196	22	)	)	PUNCT
eurjchem-365	196	23	(	(	PUNCT
eurjchem-365	196	24	oxazinone	oxazinone	NOUN
eurjchem-365	196	25	)	)	PUNCT
eurjchem-365	196	26	,	,	PUNCT
eurjchem-365	196	27	1695	1695	NUM
eurjchem-365	196	28	(c	(c	NOUN
eurjchem-365	196	29	=	=	SYM
eurjchem-365	196	30	o	o	NOUN
eurjchem-365	196	31	)	)	PUNCT
eurjchem-365	196	32	(	(	PUNCT
eurjchem-365	196	33	amide	amide	NOUN
eurjchem-365	196	34	)	)	PUNCT
eurjchem-365	196	35	.	.	PUNCT
eurjchem-365	197	1	1h	1h	NUM
eurjchem-365	197	2	nmr	nmr	NOUN
eurjchem-365	197	3	(	(	PUNCT
eurjchem-365	197	4	300	300	NUM
eurjchem-365	197	5	mhz	mhz	NOUN
eurjchem-365	197	6	,	,	PUNCT
eurjchem-365	197	7	dmso‐d6	dmso‐d6	NUM
eurjchem-365	197	8	):	):	PUNCT
eurjchem-365	197	9	7.03‐8.10	7.03‐8.10	NUM
eurjchem-365	197	10	(	(	PUNCT
eurjchem-365	197	11	m	m	PROPN
eurjchem-365	197	12	,	,	PUNCT
eurjchem-365	197	13	13	13	NUM
eurjchem-365	197	14	h	h	NOUN
eurjchem-365	197	15	,	,	PUNCT
eurjchem-365	197	16	ar‐h	ar‐h	NOUN
eurjchem-365	197	17	)	)	PUNCT
eurjchem-365	197	18	,	,	PUNCT
eurjchem-365	197	19	8.21	8.21	NUM
eurjchem-365	197	20	(	(	PUNCT
eurjchem-365	197	21	s	s	PROPN
eurjchem-365	197	22	,	,	PUNCT
eurjchem-365	197	23	1h	1h	NUM
eurjchem-365	197	24	,	,	PUNCT
eurjchem-365	197	25	cn‐c	cn‐c	NOUN
eurjchem-365	197	26	=	=	SYM
eurjchem-365	197	27	ch	ch	NOUN
eurjchem-365	197	28	)	)	PUNCT
eurjchem-365	197	29	,	,	PUNCT
eurjchem-365	197	30	10.23	10.23	NUM
eurjchem-365	197	31	(	(	PUNCT
eurjchem-365	197	32	s	s	PROPN
eurjchem-365	197	33	,	,	PUNCT
eurjchem-365	197	34	1h	1h	NUM
eurjchem-365	197	35	,	,	PUNCT
eurjchem-365	197	36	nh	nh	PROPN
eurjchem-365	197	37	)	)	PUNCT
eurjchem-365	197	38	.	.	PUNCT
eurjchem-365	198	1	ms	ms	NOUN
eurjchem-365	198	2	(	(	PUNCT
eurjchem-365	198	3	ei	ei	PROPN
eurjchem-365	198	4	,	,	PUNCT
eurjchem-365	198	5	m	m	PROPN
eurjchem-365	198	6	/	/	SYM
eurjchem-365	198	7	z	z	NOUN
eurjchem-365	198	8	):	):	PUNCT
eurjchem-365	198	9	393	393	NUM
eurjchem-365	198	10	(	(	PUNCT
eurjchem-365	198	11	m.+	m.+	NOUN
eurjchem-365	198	12	)	)	PUNCT
eurjchem-365	198	13	.	.	PUNCT
eurjchem-365	199	1	anal	anal	PROPN
eurjchem-365	199	2	.	.	PUNCT
eurjchem-365	199	3	calcd	calcd	NOUN
eurjchem-365	199	4	.	.	PUNCT
eurjchem-365	200	1	for	for	ADP
eurjchem-365	200	2	c24h15n3o3	c24h15n3o3	NOUN
eurjchem-365	200	3	:	:	PUNCT
eurjchem-365	200	4	c	c	X
eurjchem-365	200	5	,	,	PUNCT
eurjchem-365	200	6	73.28	73.28	NUM
eurjchem-365	200	7	;	;	PUNCT
eurjchem-365	200	8	h	h	NOUN
eurjchem-365	200	9	,	,	PUNCT
eurjchem-365	200	10	3.84	3.84	NUM
eurjchem-365	200	11	;	;	PUNCT
eurjchem-365	200	12	n	n	CCONJ
eurjchem-365	200	13	,	,	PUNCT
eurjchem-365	200	14	10.68	10.68	NUM
eurjchem-365	200	15	.	.	PUNCT
eurjchem-365	200	16	found	find	VERB
eurjchem-365	200	17	:	:	PUNCT
eurjchem-365	201	1	c	c	X
eurjchem-365	201	2	,	,	PUNCT
eurjchem-365	201	3	73.42	73.42	NUM
eurjchem-365	201	4	;	;	PUNCT
eurjchem-365	201	5	h	h	NOUN
eurjchem-365	201	6	,	,	PUNCT
eurjchem-365	201	7	3.61	3.61	NUM
eurjchem-365	201	8	;	;	PUNCT
eurjchem-365	201	9	n	n	CCONJ
eurjchem-365	201	10	,	,	PUNCT
eurjchem-365	201	11	10.55	10.55	NUM
eurjchem-365	201	12	%	%	NOUN
eurjchem-365	201	13	.	.	PUNCT
eurjchem-365	202	1	2.10	2.10	NUM
eurjchem-365	202	2	.	.	PUNCT
eurjchem-365	203	1	n‐[2‐(2‐benzylidenehydrazinecarbonyl)phenyl]‐2‐	n‐[2‐(2‐benzylidenehydrazinecarbonyl)phenyl]‐2‐	NUM
eurjchem-365	203	2	cyanoacetamide	cyanoacetamide	ADJ
eurjchem-365	203	3	(	(	PUNCT
eurjchem-365	203	4	15	15	NUM
eurjchem-365	203	5	)	)	PUNCT
eurjchem-365	203	6	a	a	DET
eurjchem-365	203	7	mixture	mixture	NOUN
eurjchem-365	203	8	of	of	ADP
eurjchem-365	203	9	benzoxazinone	benzoxazinone	NOUN
eurjchem-365	203	10	10	10	NUM
eurjchem-365	203	11	(	(	PUNCT
eurjchem-365	203	12	1.49	1.49	NUM
eurjchem-365	203	13	g	g	NOUN
eurjchem-365	203	14	;	;	PUNCT
eurjchem-365	203	15	5	5	NUM
eurjchem-365	203	16	mmol	mmol	NOUN
eurjchem-365	203	17	)	)	PUNCT
eurjchem-365	203	18	and	and	CCONJ
eurjchem-365	203	19	hydrazine	hydrazine	NOUN
eurjchem-365	203	20	hydrate	hydrate	NOUN
eurjchem-365	203	21	(	(	PUNCT
eurjchem-365	203	22	0.1	0.1	NUM
eurjchem-365	203	23	ml	ml	NOUN
eurjchem-365	203	24	,	,	PUNCT
eurjchem-365	203	25	5	5	NUM
eurjchem-365	203	26	mmol	mmol	NOUN
eurjchem-365	203	27	)	)	PUNCT
eurjchem-365	203	28	in	in	ADP
eurjchem-365	203	29	ethanol	ethanol	NOUN
eurjchem-365	203	30	(	(	PUNCT
eurjchem-365	203	31	50	50	NUM
eurjchem-365	203	32	ml	ml	NOUN
eurjchem-365	203	33	)	)	PUNCT
eurjchem-365	203	34	was	be	AUX
eurjchem-365	203	35	refluxed	refluxe	VERB
eurjchem-365	203	36	for	for	ADP
eurjchem-365	203	37	3	3	NUM
eurjchem-365	203	38	h.	h.	NOUN
eurjchem-365	203	39	the	the	DET
eurjchem-365	203	40	solid	solid	ADV
eurjchem-365	203	41	separated	separate	VERB
eurjchem-365	203	42	after	after	ADP
eurjchem-365	203	43	concentration	concentration	NOUN
eurjchem-365	203	44	was	be	AUX
eurjchem-365	203	45	collected	collect	VERB
eurjchem-365	203	46	and	and	CCONJ
eurjchem-365	203	47	crystallized	crystallize	VERB
eurjchem-365	203	48	from	from	ADP
eurjchem-365	203	49	ethanol	ethanol	NOUN
eurjchem-365	203	50	to	to	PART
eurjchem-365	203	51	yield	yield	VERB
eurjchem-365	203	52	15	15	NUM
eurjchem-365	203	53	as	as	ADP
eurjchem-365	203	54	pale	pale	ADJ
eurjchem-365	203	55	yellow	yellow	ADJ
eurjchem-365	203	56	crystals	crystal	NOUN
eurjchem-365	203	57	(	(	PUNCT
eurjchem-365	203	58	scheme	scheme	NOUN
eurjchem-365	203	59	1	1	NUM
eurjchem-365	203	60	)	)	PUNCT
eurjchem-365	203	61	.	.	PUNCT
eurjchem-365	204	1	yield	yield	NOUN
eurjchem-365	204	2	:	:	PUNCT
eurjchem-365	204	3	55	55	NUM
eurjchem-365	204	4	%	%	NOUN
eurjchem-365	204	5	.	.	PUNCT
eurjchem-365	205	1	m.p	m.p	PROPN
eurjchem-365	205	2	.	.	PROPN
eurjchem-365	205	3	:	:	PUNCT
eurjchem-365	206	1	140‐142	140‐142	NUM
eurjchem-365	206	2	oc	oc	PROPN
eurjchem-365	206	3	.	.	PUNCT
eurjchem-365	206	4	ft‐ir	ft‐ir	NOUN
eurjchem-365	206	5	(	(	PUNCT
eurjchem-365	206	6	kbr	kbr	PROPN
eurjchem-365	206	7	,	,	PUNCT
eurjchem-365	206	8	cm‐1	cm‐1	PROPN
eurjchem-365	206	9	):	):	PUNCT
eurjchem-365	206	10	3240	3240	NUM
eurjchem-365	206	11	,	,	PUNCT
eurjchem-365	206	12	3192	3192	NUM
eurjchem-365	206	13	(nh	(nh	PROPN
eurjchem-365	206	14	)	)	PUNCT
eurjchem-365	206	15	,	,	PUNCT
eurjchem-365	206	16	2212	2212	NUM
eurjchem-365	206	17	(cn	(cn	NOUN
eurjchem-365	206	18	)	)	PUNCT
eurjchem-365	206	19	,	,	PUNCT
eurjchem-365	206	20	1696	1696	NUM
eurjchem-365	206	21	(c	(c	PROPN
eurjchem-365	206	22	=	=	SYM
eurjchem-365	206	23	o	o	NOUN
eurjchem-365	206	24	)	)	PUNCT
eurjchem-365	206	25	(	(	PUNCT
eurjchem-365	206	26	amide	amide	NOUN
eurjchem-365	206	27	)	)	PUNCT
eurjchem-365	206	28	.	.	PUNCT
eurjchem-365	207	1	1h	1h	NUM
eurjchem-365	207	2	nmr	nmr	NOUN
eurjchem-365	207	3	(	(	PUNCT
eurjchem-365	207	4	300	300	NUM
eurjchem-365	207	5	mhz	mhz	NOUN
eurjchem-365	207	6	,	,	PUNCT
eurjchem-365	207	7	dmso‐d6	dmso‐d6	NUM
eurjchem-365	207	8	):	):	PUNCT
eurjchem-365	207	9	3.91	3.91	NUM
eurjchem-365	207	10	(	(	PUNCT
eurjchem-365	207	11	s	s	PROPN
eurjchem-365	207	12	,	,	PUNCT
eurjchem-365	207	13	2h	2h	NUM
eurjchem-365	207	14	,	,	PUNCT
eurjchem-365	207	15	ch2‐cn	ch2‐cn	NOUN
eurjchem-365	207	16	)	)	PUNCT
eurjchem-365	207	17	,	,	PUNCT
eurjchem-365	207	18	7.30‐8.49	7.30‐8.49	NUM
eurjchem-365	207	19	(	(	PUNCT
eurjchem-365	207	20	m	m	PROPN
eurjchem-365	207	21	,	,	PUNCT
eurjchem-365	207	22	10	10	NUM
eurjchem-365	207	23	h	h	NOUN
eurjchem-365	207	24	,	,	PUNCT
eurjchem-365	207	25	=	=	NOUN
eurjchem-365	207	26	ch	ch	NOUN
eurjchem-365	207	27	,	,	PUNCT
eurjchem-365	207	28	ar‐h	ar‐h	PROPN
eurjchem-365	207	29	)	)	PUNCT
eurjchem-365	207	30	,	,	PUNCT
eurjchem-365	207	31	11.49	11.49	NUM
eurjchem-365	207	32	(	(	PUNCT
eurjchem-365	207	33	br	br	PROPN
eurjchem-365	207	34	s	s	PROPN
eurjchem-365	207	35	,	,	PUNCT
eurjchem-365	207	36	1h	1h	NUM
eurjchem-365	207	37	,	,	PUNCT
eurjchem-365	207	38	2nh	2nh	NOUN
eurjchem-365	207	39	)	)	PUNCT
eurjchem-365	207	40	.	.	PUNCT
eurjchem-365	208	1	ms	ms	NOUN
eurjchem-365	208	2	(	(	PUNCT
eurjchem-365	208	3	ei	ei	PROPN
eurjchem-365	208	4	,	,	PUNCT
eurjchem-365	208	5	m	m	PROPN
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eurjchem-365	208	7	z	z	NOUN
eurjchem-365	208	8	):	):	PUNCT
eurjchem-365	208	9	306	306	NUM
eurjchem-365	208	10	(	(	PUNCT
eurjchem-365	208	11	m.+	m.+	NOUN
eurjchem-365	208	12	)	)	PUNCT
eurjchem-365	208	13	.	.	PUNCT
eurjchem-365	209	1	anal	anal	PROPN
eurjchem-365	209	2	.	.	PUNCT
eurjchem-365	209	3	calcd	calcd	NOUN
eurjchem-365	209	4	.	.	PUNCT
eurjchem-365	210	1	for	for	SCONJ
eurjchem-365	210	2	c17h14n4o2	c17h14n4o2	PROPN
eurjchem-365	210	3	:	:	PUNCT
eurjchem-365	210	4	c	c	X
eurjchem-365	210	5	,	,	PUNCT
eurjchem-365	210	6	66.60	66.60	NUM
eurjchem-365	210	7	;	;	PUNCT
eurjchem-365	210	8	h	h	NOUN
eurjchem-365	210	9	,	,	PUNCT
eurjchem-365	210	10	4.60	4.60	NUM
eurjchem-365	210	11	;	;	PUNCT
eurjchem-365	210	12	n	n	CCONJ
eurjchem-365	210	13	,	,	PUNCT
eurjchem-365	210	14	18.28	18.28	NUM
eurjchem-365	210	15	.	.	PUNCT
eurjchem-365	210	16	found	find	VERB
eurjchem-365	210	17	:	:	PUNCT
eurjchem-365	211	1	c	c	X
eurjchem-365	211	2	,	,	PUNCT
eurjchem-365	211	3	66.33	66.33	NUM
eurjchem-365	211	4	;	;	PUNCT
eurjchem-365	212	1	h	h	X
eurjchem-365	212	2	,	,	PUNCT
eurjchem-365	212	3	4.72	4.72	NUM
eurjchem-365	212	4	;	;	PUNCT
eurjchem-365	212	5	n	n	CCONJ
eurjchem-365	212	6	,	,	PUNCT
eurjchem-365	212	7	18.01	18.01	NUM
eurjchem-365	212	8	%	%	NOUN
eurjchem-365	212	9	.	.	PUNCT
eurjchem-365	213	1	2.11	2.11	NUM
eurjchem-365	213	2	.	.	PUNCT
eurjchem-365	214	1	2‐oxo‐4‐phenyl‐2h‐pyrido[1,2‐a]pyrimidine‐3‐	2‐oxo‐4‐phenyl‐2h‐pyrido[1,2‐a]pyrimidine‐3‐	NUM
eurjchem-365	214	2	carbonitrile	carbonitrile	NOUN
eurjchem-365	214	3	(	(	PUNCT
eurjchem-365	214	4	16	16	NUM
eurjchem-365	214	5	)	)	PUNCT
eurjchem-365	214	6	to	to	ADP
eurjchem-365	214	7	a	a	DET
eurjchem-365	214	8	solution	solution	NOUN
eurjchem-365	214	9	of	of	ADP
eurjchem-365	214	10	1	1	NUM
eurjchem-365	214	11	(	(	PUNCT
eurjchem-365	214	12	1.9	1.9	NUM
eurjchem-365	214	13	g	g	NOUN
eurjchem-365	214	14	;	;	PUNCT
eurjchem-365	214	15	10	10	NUM
eurjchem-365	214	16	mmol	mmol	NOUN
eurjchem-365	214	17	)	)	PUNCT
eurjchem-365	214	18	in	in	ADP
eurjchem-365	214	19	dry	dry	ADJ
eurjchem-365	214	20	benzene	benzene	NOUN
eurjchem-365	214	21	(	(	PUNCT
eurjchem-365	214	22	30	30	NUM
eurjchem-365	214	23	ml	ml	NOUN
eurjchem-365	214	24	)	)	PUNCT
eurjchem-365	214	25	in	in	ADP
eurjchem-365	214	26	presence	presence	NOUN
eurjchem-365	214	27	of	of	ADP
eurjchem-365	214	28	triethylamine	triethylamine	NOUN
eurjchem-365	214	29	(	(	PUNCT
eurjchem-365	214	30	1.38	1.38	NUM
eurjchem-365	214	31	ml	ml	NOUN
eurjchem-365	214	32	;	;	PUNCT
eurjchem-365	214	33	10	10	NUM
eurjchem-365	214	34	mmol	mmol	NOUN
eurjchem-365	214	35	)	)	PUNCT
eurjchem-365	214	36	,	,	PUNCT
eurjchem-365	214	37	2‐	2‐	NUM
eurjchem-365	214	38	aminopyridine	aminopyridine	NOUN
eurjchem-365	214	39	(	(	PUNCT
eurjchem-365	214	40	0.9	0.9	NUM
eurjchem-365	214	41	g	g	NOUN
eurjchem-365	214	42	;	;	PUNCT
eurjchem-365	214	43	10	10	NUM
eurjchem-365	214	44	mmol	mmol	NOUN
eurjchem-365	214	45	)	)	PUNCT
eurjchem-365	214	46	was	be	AUX
eurjchem-365	214	47	added	add	VERB
eurjchem-365	214	48	.	.	PUNCT
eurjchem-365	215	1	the	the	DET
eurjchem-365	215	2	reaction	reaction	NOUN
eurjchem-365	215	3	mixture	mixture	NOUN
eurjchem-365	215	4	was	be	AUX
eurjchem-365	215	5	stirred	stir	VERB
eurjchem-365	215	6	at	at	ADP
eurjchem-365	215	7	room	room	NOUN
eurjchem-365	215	8	temperature	temperature	NOUN
eurjchem-365	215	9	for	for	ADP
eurjchem-365	215	10	1	1	NUM
eurjchem-365	215	11	h.	h.	NOUN
eurjchem-365	215	12	the	the	DET
eurjchem-365	215	13	semisolid	semisolid	NOUN
eurjchem-365	215	14	produced	produce	VERB
eurjchem-365	215	15	was	be	AUX
eurjchem-365	215	16	collected	collect	VERB
eurjchem-365	215	17	,	,	PUNCT
eurjchem-365	215	18	washed	wash	VERB
eurjchem-365	215	19	with	with	ADP
eurjchem-365	215	20	water	water	NOUN
eurjchem-365	215	21	several	several	ADJ
eurjchem-365	215	22	times	time	NOUN
eurjchem-365	215	23	,	,	PUNCT
eurjchem-365	215	24	and	and	CCONJ
eurjchem-365	215	25	then	then	ADV
eurjchem-365	215	26	triturated	triturate	VERB
eurjchem-365	215	27	with	with	ADP
eurjchem-365	215	28	methyl	methyl	NOUN
eurjchem-365	215	29	alcohol	alcohol	NOUN
eurjchem-365	215	30	.	.	PUNCT
eurjchem-365	216	1	the	the	DET
eurjchem-365	216	2	solid	solid	ADJ
eurjchem-365	216	3	separated	separate	VERB
eurjchem-365	216	4	was	be	AUX
eurjchem-365	216	5	collected	collect	VERB
eurjchem-365	216	6	,	,	PUNCT
eurjchem-365	216	7	dried	dry	VERB
eurjchem-365	216	8	and	and	CCONJ
eurjchem-365	216	9	crystallized	crystallize	VERB
eurjchem-365	216	10	from	from	ADP
eurjchem-365	216	11	methanol	methanol	NOUN
eurjchem-365	216	12	to	to	PART
eurjchem-365	216	13	afford	afford	VERB
eurjchem-365	216	14	16	16	NUM
eurjchem-365	216	15	as	as	ADP
eurjchem-365	216	16	colourless	colourless	ADJ
eurjchem-365	216	17	crystals	crystal	NOUN
eurjchem-365	216	18	.	.	PUNCT
eurjchem-365	217	1	yield	yield	NOUN
eurjchem-365	217	2	:	:	PUNCT
eurjchem-365	217	3	40	40	NUM
eurjchem-365	217	4	%	%	NOUN
eurjchem-365	217	5	.	.	PUNCT
eurjchem-365	218	1	m.p	m.p	PROPN
eurjchem-365	218	2	.	.	PROPN
eurjchem-365	218	3	:	:	PUNCT
eurjchem-365	219	1	203‐205	203‐205	NUM
eurjchem-365	219	2	oc	oc	PROPN
eurjchem-365	219	3	.	.	PUNCT
eurjchem-365	219	4	ft‐ir	ft‐ir	NOUN
eurjchem-365	219	5	(	(	PUNCT
eurjchem-365	219	6	kbr	kbr	PROPN
eurjchem-365	219	7	,	,	PUNCT
eurjchem-365	219	8	cm‐1	cm‐1	PROPN
eurjchem-365	219	9	):	):	PUNCT
eurjchem-365	219	10	2218	2218	NUM
eurjchem-365	219	11	(cn	(cn	NOUN
eurjchem-365	219	12	)	)	PUNCT
eurjchem-365	219	13	,	,	PUNCT
eurjchem-365	219	14	1705	1705	NUM
eurjchem-365	219	15	(c	(c	PROPN
eurjchem-365	219	16	=	=	SYM
eurjchem-365	219	17	o	o	NOUN
eurjchem-365	219	18	)	)	PUNCT
eurjchem-365	219	19	(	(	PUNCT
eurjchem-365	219	20	cyclic	cyclic	ADJ
eurjchem-365	219	21	amide	amide	NOUN
eurjchem-365	219	22	)	)	PUNCT
eurjchem-365	219	23	.	.	PUNCT
eurjchem-365	220	1	1h	1h	NUM
eurjchem-365	220	2	nmr	nmr	NOUN
eurjchem-365	220	3	(	(	PUNCT
eurjchem-365	220	4	300	300	NUM
eurjchem-365	220	5	mhz	mhz	NOUN
eurjchem-365	220	6	,	,	PUNCT
eurjchem-365	220	7	dmso‐d6	dmso‐d6	NUM
eurjchem-365	220	8	):	):	PUNCT
eurjchem-365	220	9	7.59‐9.80	7.59‐9.80	NUM
eurjchem-365	220	10	(	(	PUNCT
eurjchem-365	220	11	m	m	PROPN
eurjchem-365	220	12	,	,	PUNCT
eurjchem-365	220	13	9	9	NUM
eurjchem-365	220	14	h	h	NOUN
eurjchem-365	220	15	,	,	PUNCT
eurjchem-365	220	16	ar‐h	ar‐h	NOUN
eurjchem-365	220	17	)	)	PUNCT
eurjchem-365	220	18	.	.	PUNCT
eurjchem-365	221	1	ms	ms	NOUN
eurjchem-365	221	2	(	(	PUNCT
eurjchem-365	221	3	ei	ei	PROPN
eurjchem-365	221	4	,	,	PUNCT
eurjchem-365	221	5	m	m	PROPN
eurjchem-365	221	6	/	/	SYM
eurjchem-365	221	7	z	z	NOUN
eurjchem-365	221	8	):	):	PUNCT
eurjchem-365	221	9	247	247	NUM
eurjchem-365	221	10	(	(	PUNCT
eurjchem-365	221	11	m.+	m.+	NOUN
eurjchem-365	221	12	)	)	PUNCT
eurjchem-365	221	13	.	.	PUNCT
eurjchem-365	222	1	anal	anal	PROPN
eurjchem-365	222	2	.	.	PUNCT
eurjchem-365	222	3	calcd	calcd	NOUN
eurjchem-365	222	4	.	.	PUNCT
eurjchem-365	223	1	for	for	SCONJ
eurjchem-365	223	2	c15h9n3o	c15h9n3o	NOUN
eurjchem-365	223	3	:	:	PUNCT
eurjchem-365	223	4	c	c	X
eurjchem-365	223	5	,	,	PUNCT
eurjchem-365	223	6	72.87	72.87	NUM
eurjchem-365	223	7	;	;	PUNCT
eurjchem-365	223	8	h	h	NOUN
eurjchem-365	223	9	,	,	PUNCT
eurjchem-365	223	10	3.64	3.64	NUM
eurjchem-365	223	11	;	;	PUNCT
eurjchem-365	223	12	n	n	CCONJ
eurjchem-365	223	13	,	,	PUNCT
eurjchem-365	223	14	17.01	17.01	NUM
eurjchem-365	223	15	.	.	PUNCT
eurjchem-365	223	16	found	find	VERB
eurjchem-365	223	17	:	:	PUNCT
eurjchem-365	224	1	c	c	X
eurjchem-365	224	2	,	,	PUNCT
eurjchem-365	224	3	72.43	72.43	NUM
eurjchem-365	224	4	;	;	PUNCT
eurjchem-365	225	1	h	h	NOUN
eurjchem-365	225	2	,	,	PUNCT
eurjchem-365	225	3	3.71	3.71	NUM
eurjchem-365	225	4	;	;	PUNCT
eurjchem-365	225	5	n	n	CCONJ
eurjchem-365	225	6	,	,	PUNCT
eurjchem-365	225	7	17.23	17.23	NUM
eurjchem-365	225	8	%	%	NOUN
eurjchem-365	225	9	.	.	PUNCT
eurjchem-365	226	1	2.12	2.12	NUM
eurjchem-365	226	2	.	.	NUM
eurjchem-365	226	3	2‐(1‐cyano‐2‐phenyl‐ethen‐1‐yl)‐5‐phenyl‐1,3,4‐	2‐(1‐cyano‐2‐phenyl‐ethen‐1‐yl)‐5‐phenyl‐1,3,4‐	NUM
eurjchem-365	226	4	oxadiazole	oxadiazole	NOUN
eurjchem-365	226	5	(	(	PUNCT
eurjchem-365	226	6	19	19	NUM
eurjchem-365	226	7	)	)	PUNCT
eurjchem-365	226	8	a	a	DET
eurjchem-365	226	9	solution	solution	NOUN
eurjchem-365	226	10	of	of	ADP
eurjchem-365	226	11	(	(	PUNCT
eurjchem-365	226	12	18	18	NUM
eurjchem-365	226	13	)	)	PUNCT
eurjchem-365	226	14	(	(	PUNCT
eurjchem-365	226	15	1	1	NUM
eurjchem-365	226	16	g	g	NOUN
eurjchem-365	226	17	)	)	PUNCT
eurjchem-365	226	18	in	in	ADP
eurjchem-365	226	19	phosphorous	phosphorous	ADJ
eurjchem-365	226	20	oxychloride	oxychloride	NOUN
eurjchem-365	226	21	(	(	PUNCT
eurjchem-365	226	22	20	20	NUM
eurjchem-365	226	23	ml	ml	NOUN
eurjchem-365	226	24	)	)	PUNCT
eurjchem-365	226	25	was	be	AUX
eurjchem-365	226	26	heated	heat	VERB
eurjchem-365	226	27	on	on	ADP
eurjchem-365	226	28	water	water	NOUN
eurjchem-365	226	29	bath	bath	NOUN
eurjchem-365	226	30	for	for	ADP
eurjchem-365	226	31	4	4	NUM
eurjchem-365	226	32	h.	h.	NOUN
eurjchem-365	226	33	the	the	DET
eurjchem-365	226	34	reaction	reaction	NOUN
eurjchem-365	226	35	mixture	mixture	NOUN
eurjchem-365	226	36	was	be	AUX
eurjchem-365	226	37	left	leave	VERB
eurjchem-365	226	38	to	to	PART
eurjchem-365	226	39	cool	cool	ADJ
eurjchem-365	226	40	,	,	PUNCT
eurjchem-365	226	41	and	and	CCONJ
eurjchem-365	226	42	then	then	ADV
eurjchem-365	226	43	poured	pour	VERB
eurjchem-365	226	44	with	with	ADP
eurjchem-365	226	45	stirring	stir	VERB
eurjchem-365	226	46	into	into	ADP
eurjchem-365	226	47	crushed	crush	VERB
eurjchem-365	226	48	ice	ice	NOUN
eurjchem-365	226	49	.	.	PUNCT
eurjchem-365	227	1	the	the	DET
eurjchem-365	227	2	solid	solid	ADJ
eurjchem-365	227	3	separated	separate	VERB
eurjchem-365	227	4	out	out	ADP
eurjchem-365	227	5	was	be	AUX
eurjchem-365	227	6	filtered	filter	VERB
eurjchem-365	227	7	off	off	ADP
eurjchem-365	227	8	,	,	PUNCT
eurjchem-365	227	9	washed	wash	VERB
eurjchem-365	227	10	with	with	ADP
eurjchem-365	227	11	water	water	NOUN
eurjchem-365	227	12	several	several	ADJ
eurjchem-365	227	13	times	time	NOUN
eurjchem-365	227	14	,	,	PUNCT
eurjchem-365	227	15	dried	dry	VERB
eurjchem-365	227	16	and	and	CCONJ
eurjchem-365	227	17	crystallized	crystallize	VERB
eurjchem-365	227	18	from	from	ADP
eurjchem-365	227	19	ethanol	ethanol	NOUN
eurjchem-365	227	20	to	to	PART
eurjchem-365	227	21	yield	yield	VERB
eurjchem-365	227	22	19	19	NUM
eurjchem-365	227	23	as	as	ADP
eurjchem-365	227	24	colourless	colourless	ADJ
eurjchem-365	227	25	crystals	crystal	NOUN
eurjchem-365	227	26	(	(	PUNCT
eurjchem-365	227	27	scheme	scheme	NOUN
eurjchem-365	227	28	1	1	NUM
eurjchem-365	227	29	)	)	PUNCT
eurjchem-365	227	30	.	.	PUNCT
eurjchem-365	228	1	yield	yield	NOUN
eurjchem-365	228	2	:	:	PUNCT
eurjchem-365	228	3	40	40	NUM
eurjchem-365	228	4	%	%	NOUN
eurjchem-365	228	5	.	.	PUNCT
eurjchem-365	229	1	m.p	m.p	PROPN
eurjchem-365	229	2	.	.	PROPN
eurjchem-365	229	3	:	:	PUNCT
eurjchem-365	230	1	168‐170	168‐170	NUM
eurjchem-365	230	2	oc	oc	PROPN
eurjchem-365	230	3	.	.	PUNCT
eurjchem-365	230	4	ft‐ir	ft‐ir	NOUN
eurjchem-365	230	5	(	(	PUNCT
eurjchem-365	230	6	kbr	kbr	PROPN
eurjchem-365	230	7	,	,	PUNCT
eurjchem-365	230	8	cm‐1	cm‐1	PROPN
eurjchem-365	230	9	):	):	PUNCT
eurjchem-365	230	10	2222	2222	NUM
eurjchem-365	230	11	(cn	(cn	NOUN
eurjchem-365	230	12	)	)	PUNCT
eurjchem-365	230	13	.	.	PUNCT
eurjchem-365	231	1	1h	1h	NUM
eurjchem-365	231	2	nmr	nmr	NOUN
eurjchem-365	231	3	(	(	PUNCT
eurjchem-365	231	4	300	300	NUM
eurjchem-365	231	5	mhz	mhz	NOUN
eurjchem-365	231	6	,	,	PUNCT
eurjchem-365	231	7	dmso‐d6	dmso‐d6	NUM
eurjchem-365	231	8	):	):	PUNCT
eurjchem-365	231	9	7.62‐8.15	7.62‐8.15	NUM
eurjchem-365	231	10	(	(	PUNCT
eurjchem-365	231	11	m	m	PROPN
eurjchem-365	231	12	,	,	PUNCT
eurjchem-365	231	13	10h	10h	NUM
eurjchem-365	231	14	,	,	PUNCT
eurjchem-365	231	15	ar‐h	ar‐h	PROPN
eurjchem-365	231	16	)	)	PUNCT
eurjchem-365	231	17	,	,	PUNCT
eurjchem-365	231	18	8.53	8.53	NUM
eurjchem-365	231	19	(	(	PUNCT
eurjchem-365	231	20	s	s	PROPN
eurjchem-365	231	21	,	,	PUNCT
eurjchem-365	231	22	1h	1h	NUM
eurjchem-365	231	23	,	,	PUNCT
eurjchem-365	231	24	=	=	NOUN
eurjchem-365	231	25	ch	ch	NOUN
eurjchem-365	231	26	)	)	PUNCT
eurjchem-365	231	27	.	.	PUNCT
eurjchem-365	232	1	ms	ms	NOUN
eurjchem-365	232	2	(	(	PUNCT
eurjchem-365	232	3	ei	ei	PROPN
eurjchem-365	232	4	,	,	PUNCT
eurjchem-365	232	5	m	m	PROPN
eurjchem-365	232	6	/	/	SYM
eurjchem-365	232	7	z	z	NOUN
eurjchem-365	232	8	):	):	PUNCT
eurjchem-365	232	9	273	273	NUM
eurjchem-365	232	10	(	(	PUNCT
eurjchem-365	232	11	m.+	m.+	NOUN
eurjchem-365	232	12	)	)	PUNCT
eurjchem-365	232	13	.	.	PUNCT
eurjchem-365	233	1	anal	anal	PROPN
eurjchem-365	233	2	.	.	PUNCT
eurjchem-365	233	3	calcd	calcd	NOUN
eurjchem-365	233	4	.	.	PUNCT
eurjchem-365	234	1	for	for	ADP
eurjchem-365	234	2	c17h11n3o	c17h11n3o	NOUN
eurjchem-365	234	3	:	:	PUNCT
eurjchem-365	234	4	c	c	X
eurjchem-365	234	5	,	,	PUNCT
eurjchem-365	234	6	74.72	74.72	NUM
eurjchem-365	234	7	;	;	PUNCT
eurjchem-365	234	8	h	h	NOUN
eurjchem-365	234	9	,	,	PUNCT
eurjchem-365	234	10	4.02	4.02	NUM
eurjchem-365	234	11	;	;	PUNCT
eurjchem-365	234	12	n	n	CCONJ
eurjchem-365	234	13	,	,	PUNCT
eurjchem-365	234	14	15.38	15.38	NUM
eurjchem-365	234	15	.	.	PUNCT
eurjchem-365	234	16	found	find	VERB
eurjchem-365	234	17	:	:	PUNCT
eurjchem-365	235	1	c	c	X
eurjchem-365	235	2	,	,	PUNCT
eurjchem-365	235	3	74.98	74.98	NUM
eurjchem-365	235	4	;	;	PUNCT
eurjchem-365	235	5	h	h	NOUN
eurjchem-365	235	6	,	,	PUNCT
eurjchem-365	235	7	4.22	4.22	NUM
eurjchem-365	235	8	;	;	PUNCT
eurjchem-365	235	9	n	n	CCONJ
eurjchem-365	235	10	,	,	PUNCT
eurjchem-365	235	11	15.46	15.46	NUM
eurjchem-365	235	12	%	%	NOUN
eurjchem-365	235	13	.	.	PUNCT
eurjchem-365	236	1	2.13	2.13	NUM
eurjchem-365	236	2	.	.	X
eurjchem-365	237	1	2‐(1‐cyano‐2‐phenyl‐ethen‐1‐yl)benzo[d]oxazole	2‐(1‐cyano‐2‐phenyl‐ethen‐1‐yl)benzo[d]oxazole	NUM
eurjchem-365	237	2	(	(	PUNCT
eurjchem-365	237	3	21	21	NUM
eurjchem-365	237	4	)	)	PUNCT
eurjchem-365	237	5	a	a	DET
eurjchem-365	237	6	solution	solution	NOUN
eurjchem-365	237	7	of	of	ADP
eurjchem-365	237	8	20	20	NUM
eurjchem-365	237	9	(	(	PUNCT
eurjchem-365	237	10	1	1	NUM
eurjchem-365	237	11	g	g	NOUN
eurjchem-365	237	12	)	)	PUNCT
eurjchem-365	237	13	in	in	ADP
eurjchem-365	237	14	phosphorous	phosphorous	ADJ
eurjchem-365	237	15	oxychloride	oxychloride	NOUN
eurjchem-365	237	16	(	(	PUNCT
eurjchem-365	237	17	20	20	NUM
eurjchem-365	237	18	ml	ml	NOUN
eurjchem-365	237	19	)	)	PUNCT
eurjchem-365	237	20	was	be	AUX
eurjchem-365	237	21	heated	heat	VERB
eurjchem-365	237	22	on	on	ADP
eurjchem-365	237	23	water	water	NOUN
eurjchem-365	237	24	bath	bath	NOUN
eurjchem-365	237	25	for	for	ADP
eurjchem-365	237	26	8	8	NUM
eurjchem-365	237	27	h.	h.	NOUN
eurjchem-365	237	28	the	the	DET
eurjchem-365	237	29	reaction	reaction	NOUN
eurjchem-365	237	30	mixture	mixture	NOUN
eurjchem-365	237	31	was	be	AUX
eurjchem-365	237	32	left	leave	VERB
eurjchem-365	237	33	to	to	PART
eurjchem-365	237	34	cool	cool	ADJ
eurjchem-365	237	35	,	,	PUNCT
eurjchem-365	237	36	and	and	CCONJ
eurjchem-365	237	37	then	then	ADV
eurjchem-365	237	38	poured	pour	VERB
eurjchem-365	237	39	into	into	ADP
eurjchem-365	237	40	crushed	crush	VERB
eurjchem-365	237	41	ice	ice	NOUN
eurjchem-365	237	42	.	.	PUNCT
eurjchem-365	238	1	the	the	DET
eurjchem-365	238	2	solid	solid	ADJ
eurjchem-365	238	3	,	,	PUNCT
eurjchem-365	238	4	which	which	PRON
eurjchem-365	238	5	separated	separate	VERB
eurjchem-365	238	6	out	out	ADP
eurjchem-365	238	7	,	,	PUNCT
eurjchem-365	238	8	was	be	AUX
eurjchem-365	238	9	filtered	filter	VERB
eurjchem-365	238	10	,	,	PUNCT
eurjchem-365	238	11	washed	wash	VERB
eurjchem-365	238	12	with	with	ADP
eurjchem-365	238	13	water	water	NOUN
eurjchem-365	238	14	several	several	ADJ
eurjchem-365	238	15	times	time	NOUN
eurjchem-365	238	16	,	,	PUNCT
eurjchem-365	238	17	dried	dry	VERB
eurjchem-365	238	18	and	and	CCONJ
eurjchem-365	238	19	crystallized	crystallize	VERB
eurjchem-365	238	20	from	from	ADP
eurjchem-365	238	21	benzene	benzene	NOUN
eurjchem-365	238	22	to	to	PART
eurjchem-365	238	23	afford	afford	VERB
eurjchem-365	238	24	21	21	NUM
eurjchem-365	238	25	as	as	ADP
eurjchem-365	238	26	yellow	yellow	ADJ
eurjchem-365	238	27	crystals	crystal	NOUN
eurjchem-365	238	28	(	(	PUNCT
eurjchem-365	238	29	scheme	scheme	NOUN
eurjchem-365	238	30	1	1	NUM
eurjchem-365	238	31	)	)	PUNCT
eurjchem-365	238	32	.	.	PUNCT
eurjchem-365	239	1	yield	yield	NOUN
eurjchem-365	239	2	:	:	PUNCT
eurjchem-365	239	3	40	40	NUM
eurjchem-365	239	4	%	%	NOUN
eurjchem-365	239	5	.	.	PUNCT
eurjchem-365	240	1	m.p	m.p	PROPN
eurjchem-365	240	2	.	.	PROPN
eurjchem-365	240	3	:	:	PUNCT
eurjchem-365	241	1	140‐142	140‐142	NUM
eurjchem-365	241	2	oc	oc	PROPN
eurjchem-365	241	3	.	.	PUNCT
eurjchem-365	241	4	ft‐ir	ft‐ir	NOUN
eurjchem-365	241	5	(	(	PUNCT
eurjchem-365	241	6	kbr	kbr	PROPN
eurjchem-365	241	7	,	,	PUNCT
eurjchem-365	241	8	cm‐1	cm‐1	PROPN
eurjchem-365	241	9	):	):	PUNCT
eurjchem-365	241	10	2226	2226	NUM
eurjchem-365	241	11	(cn	(cn	NOUN
eurjchem-365	241	12	)	)	PUNCT
eurjchem-365	241	13	.	.	PUNCT
eurjchem-365	242	1	1h	1h	NUM
eurjchem-365	242	2	nmr	nmr	NOUN
eurjchem-365	242	3	(	(	PUNCT
eurjchem-365	242	4	300	300	NUM
eurjchem-365	242	5	mhz	mhz	NOUN
eurjchem-365	242	6	,	,	PUNCT
eurjchem-365	242	7	dmso‐	dmso‐	PROPN
eurjchem-365	242	8	dmso‐d6	dmso‐d6	NUM
eurjchem-365	242	9	):	):	PUNCT
eurjchem-365	242	10	7.47‐	7.47‐	NUM
eurjchem-365	242	11	8.03	8.03	NUM
eurjchem-365	242	12	(	(	PUNCT
eurjchem-365	242	13	m	m	PROPN
eurjchem-365	242	14	,	,	PUNCT
eurjchem-365	242	15	9	9	NUM
eurjchem-365	242	16	h	h	NOUN
eurjchem-365	242	17	,	,	PUNCT
eurjchem-365	242	18	ar‐h	ar‐h	NOUN
eurjchem-365	242	19	)	)	PUNCT
eurjchem-365	242	20	,	,	PUNCT
eurjchem-365	242	21	8.52	8.52	NUM
eurjchem-365	242	22	(	(	PUNCT
eurjchem-365	242	23	s	s	PROPN
eurjchem-365	242	24	,	,	PUNCT
eurjchem-365	242	25	1h	1h	NUM
eurjchem-365	242	26	,	,	PUNCT
eurjchem-365	242	27	=	=	NOUN
eurjchem-365	242	28	ch	ch	NOUN
eurjchem-365	242	29	)	)	PUNCT
eurjchem-365	242	30	.	.	PUNCT
eurjchem-365	243	1	ms	ms	NOUN
eurjchem-365	243	2	(	(	PUNCT
eurjchem-365	243	3	ei	ei	PROPN
eurjchem-365	243	4	,	,	PUNCT
eurjchem-365	243	5	m	m	PROPN
eurjchem-365	243	6	/	/	SYM
eurjchem-365	243	7	z	z	NOUN
eurjchem-365	243	8	):	):	PUNCT
eurjchem-365	243	9	246	246	NUM
eurjchem-365	243	10	(	(	PUNCT
eurjchem-365	243	11	m.+	m.+	NOUN
eurjchem-365	243	12	)	)	PUNCT
eurjchem-365	243	13	.	.	PUNCT
eurjchem-365	244	1	anal	anal	PROPN
eurjchem-365	244	2	.	.	PUNCT
eurjchem-365	244	3	calcd	calcd	NOUN
eurjchem-365	244	4	.	.	PUNCT
eurjchem-365	245	1	for	for	ADP
eurjchem-365	245	2	c16h10n2o	c16h10n2o	NOUN
eurjchem-365	245	3	:	:	PUNCT
eurjchem-365	245	4	c	c	X
eurjchem-365	245	5	,	,	PUNCT
eurjchem-365	245	6	78.04	78.04	NUM
eurjchem-365	245	7	;	;	PUNCT
eurjchem-365	245	8	h	h	NOUN
eurjchem-365	245	9	,	,	PUNCT
eurjchem-365	245	10	4.06	4.06	NUM
eurjchem-365	245	11	;	;	PUNCT
eurjchem-365	245	12	n	n	CCONJ
eurjchem-365	245	13	,	,	PUNCT
eurjchem-365	245	14	11.38	11.38	NUM
eurjchem-365	245	15	.	.	PUNCT
eurjchem-365	246	1	found	find	VERB
eurjchem-365	246	2	:	:	PUNCT
eurjchem-365	247	1	c	c	X
eurjchem-365	247	2	,	,	PUNCT
eurjchem-365	247	3	78.11	78.11	NUM
eurjchem-365	247	4	;	;	PUNCT
eurjchem-365	247	5	h	h	NOUN
eurjchem-365	247	6	,	,	PUNCT
eurjchem-365	247	7	3.77	3.77	NUM
eurjchem-365	247	8	;	;	PUNCT
eurjchem-365	247	9	n	n	CCONJ
eurjchem-365	247	10	,	,	PUNCT
eurjchem-365	247	11	11.51	11.51	NUM
eurjchem-365	247	12	%	%	NOUN
eurjchem-365	247	13	.	.	PUNCT
eurjchem-365	248	1	3	3	X
eurjchem-365	248	2	.	.	NOUN
eurjchem-365	248	3	results	result	NOUN
eurjchem-365	248	4	and	and	CCONJ
eurjchem-365	248	5	discussions	discussion	NOUN
eurjchem-365	248	6	condensation	condensation	NOUN
eurjchem-365	248	7	of	of	ADP
eurjchem-365	248	8	1	1	NUM
eurjchem-365	248	9	with	with	ADP
eurjchem-365	248	10	benzylamine	benzylamine	NOUN
eurjchem-365	248	11	or	or	CCONJ
eurjchem-365	248	12	p‐anisidine	p‐anisidine	PUNCT
eurjchem-365	248	13	in	in	ADP
eurjchem-365	248	14	presence	presence	NOUN
eurjchem-365	248	15	of	of	ADP
eurjchem-365	248	16	triethylamine	triethylamine	NOUN
eurjchem-365	248	17	afforded	afford	VERB
eurjchem-365	248	18	the	the	DET
eurjchem-365	248	19	corresponding	correspond	VERB
eurjchem-365	248	20	2‐	2‐	NUM
eurjchem-365	248	21	propenoylamides	propenoylamide	NOUN
eurjchem-365	248	22	(	(	PUNCT
eurjchem-365	248	23	2	2	NUM
eurjchem-365	248	24	and	and	CCONJ
eurjchem-365	248	25	3	3	NUM
eurjchem-365	248	26	)	)	PUNCT
eurjchem-365	248	27	.	.	PUNCT
eurjchem-365	249	1	treatment	treatment	NOUN
eurjchem-365	249	2	of	of	ADP
eurjchem-365	249	3	3	3	NUM
eurjchem-365	249	4	with	with	ADP
eurjchem-365	249	5	anhydrous	anhydrous	ADJ
eurjchem-365	249	6	aluminium	aluminium	NOUN
eurjchem-365	249	7	chloride	chloride	NOUN
eurjchem-365	249	8	in	in	ADP
eurjchem-365	249	9	benzene	benzene	NOUN
eurjchem-365	249	10	or	or	CCONJ
eurjchem-365	249	11	chlorobenzene	chlorobenzene	NOUN
eurjchem-365	249	12	gave	give	VERB
eurjchem-365	249	13	the	the	DET
eurjchem-365	249	14	corresponding	corresponding	ADJ
eurjchem-365	249	15	unexpected	unexpected	ADJ
eurjchem-365	249	16	demethylated	demethylated	ADJ
eurjchem-365	249	17	derivative	derivative	NOUN
eurjchem-365	249	18	(	(	PUNCT
eurjchem-365	249	19	4	4	NUM
eurjchem-365	249	20	)	)	PUNCT
eurjchem-365	249	21	instead	instead	ADV
eurjchem-365	249	22	of	of	ADP
eurjchem-365	249	23	the	the	DET
eurjchem-365	249	24	expected	expect	VERB
eurjchem-365	249	25	quinolinone	quinolinone	NOUN
eurjchem-365	250	1	derivative	derivative	NOUN
eurjchem-365	250	2	[	[	X
eurjchem-365	250	3	23	23	NUM
eurjchem-365	250	4	]	]	PUNCT
eurjchem-365	250	5	(	(	PUNCT
eurjchem-365	250	6	a	a	NOUN
eurjchem-365	250	7	)	)	PUNCT
eurjchem-365	250	8	(	(	PUNCT
eurjchem-365	250	9	scheme	scheme	NOUN
eurjchem-365	250	10	1	1	NUM
eurjchem-365	250	11	)	)	PUNCT
eurjchem-365	250	12	.	.	PUNCT
eurjchem-365	251	1	esterification	esterification	NOUN
eurjchem-365	251	2	of	of	ADP
eurjchem-365	251	3	1	1	NUM
eurjchem-365	251	4	with	with	ADP
eurjchem-365	251	5	o‐cresol	o‐cresol	PUNCT
eurjchem-365	251	6	and	and	CCONJ
eurjchem-365	251	7	p‐thiocresol	p‐thiocresol	PUNCT
eurjchem-365	251	8	yielded	yield	VERB
eurjchem-365	251	9	the	the	DET
eurjchem-365	251	10	ester	ester	NOUN
eurjchem-365	251	11	and	and	CCONJ
eurjchem-365	251	12	thioester	thioester	NOUN
eurjchem-365	251	13	(	(	PUNCT
eurjchem-365	251	14	5	5	NUM
eurjchem-365	251	15	and	and	CCONJ
eurjchem-365	251	16	6	6	NUM
eurjchem-365	251	17	)	)	PUNCT
eurjchem-365	251	18	(	(	PUNCT
eurjchem-365	251	19	scheme	scheme	NOUN
eurjchem-365	251	20	1	1	NUM
eurjchem-365	251	21	)	)	PUNCT
eurjchem-365	251	22	.	.	PUNCT
eurjchem-365	252	1	on	on	ADP
eurjchem-365	252	2	the	the	DET
eurjchem-365	252	3	other	other	ADJ
eurjchem-365	252	4	hand	hand	NOUN
eurjchem-365	252	5	,	,	PUNCT
eurjchem-365	252	6	condensation	condensation	NOUN
eurjchem-365	252	7	of	of	ADP
eurjchem-365	252	8	1	1	NUM
eurjchem-365	252	9	with	with	ADP
eurjchem-365	252	10	ethanolamine	ethanolamine	NOUN
eurjchem-365	252	11	gave	give	VERB
eurjchem-365	252	12	the	the	DET
eurjchem-365	252	13	disubs‐	disubs‐	NOUN
eurjchem-365	252	14	tituted	titute	VERB
eurjchem-365	252	15	derivative	derivative	NOUN
eurjchem-365	252	16	(	(	PUNCT
eurjchem-365	252	17	7	7	NUM
eurjchem-365	252	18	)	)	PUNCT
eurjchem-365	252	19	.	.	PUNCT
eurjchem-365	253	1	furthermore	furthermore	ADV
eurjchem-365	253	2	,	,	PUNCT
eurjchem-365	253	3	reaction	reaction	NOUN
eurjchem-365	253	4	of	of	ADP
eurjchem-365	253	5	1	1	NUM
eurjchem-365	253	6	with	with	ADP
eurjchem-365	253	7	o‐	o‐	PROPN
eurjchem-365	253	8	phenylenediamine	phenylenediamine	NOUN
eurjchem-365	253	9	afforded	afford	VERB
eurjchem-365	253	10	the	the	DET
eurjchem-365	253	11	corresponding	corresponding	ADJ
eurjchem-365	253	12	diamide	diamide	NOUN
eurjchem-365	253	13	(	(	PUNCT
eurjchem-365	253	14	8)	8)	NUM
eurjchem-365	253	15	which	which	PRON
eurjchem-365	253	16	,	,	PUNCT
eurjchem-365	253	17	on	on	ADP
eurjchem-365	253	18	treatment	treatment	NOUN
eurjchem-365	253	19	with	with	ADP
eurjchem-365	253	20	pocl3	pocl3	NOUN
eurjchem-365	253	21	or	or	CCONJ
eurjchem-365	253	22	heating	heating	NOUN
eurjchem-365	253	23	at	at	ADP
eurjchem-365	253	24	its	its	PRON
eurjchem-365	253	25	melting	melting	NOUN
eurjchem-365	253	26	point	point	NOUN
eurjchem-365	253	27	,	,	PUNCT
eurjchem-365	253	28	failed	fail	VERB
eurjchem-365	253	29	to	to	PART
eurjchem-365	253	30	give	give	VERB
eurjchem-365	253	31	the	the	DET
eurjchem-365	253	32	expected	expect	VERB
eurjchem-365	253	33	benzimidazole	benzimidazole	PROPN
eurjchem-365	253	34	derivative	derivative	ADJ
eurjchem-365	253	35	(	(	PUNCT
eurjchem-365	253	36	b	b	NOUN
eurjchem-365	253	37	)	)	PUNCT
eurjchem-365	254	1	[	[	X
eurjchem-365	254	2	18	18	NUM
eurjchem-365	254	3	]	]	PUNCT
eurjchem-365	254	4	(	(	PUNCT
eurjchem-365	254	5	scheme	scheme	NOUN
eurjchem-365	254	6	1	1	NUM
eurjchem-365	254	7	)	)	PUNCT
eurjchem-365	254	8	.	.	PUNCT
eurjchem-365	255	1	the	the	DET
eurjchem-365	255	2	condensation	condensation	NOUN
eurjchem-365	255	3	product	product	NOUN
eurjchem-365	255	4	of	of	ADP
eurjchem-365	255	5	reaction	reaction	NOUN
eurjchem-365	255	6	of	of	ADP
eurjchem-365	255	7	1	1	NUM
eurjchem-365	255	8	with	with	ADP
eurjchem-365	255	9	anthranilic	anthranilic	ADJ
eurjchem-365	255	10	acid	acid	NOUN
eurjchem-365	255	11	depends	depend	VERB
eurjchem-365	255	12	upon	upon	SCONJ
eurjchem-365	255	13	both	both	CCONJ
eurjchem-365	255	14	the	the	DET
eurjchem-365	255	15	base	base	NOUN
eurjchem-365	255	16	used	use	VERB
eurjchem-365	255	17	and	and	CCONJ
eurjchem-365	255	18	reaction	reaction	NOUN
eurjchem-365	255	19	conditions	condition	NOUN
eurjchem-365	255	20	.	.	PUNCT
eurjchem-365	256	1	in	in	ADP
eurjchem-365	256	2	presence	presence	NOUN
eurjchem-365	256	3	of	of	ADP
eurjchem-365	256	4	triethylamine	triethylamine	NOUN
eurjchem-365	256	5	or	or	CCONJ
eurjchem-365	256	6	pyridine	pyridine	NOUN
eurjchem-365	256	7	at	at	ADP
eurjchem-365	256	8	room	room	NOUN
eurjchem-365	256	9	temperature	temperature	NOUN
eurjchem-365	256	10	,	,	PUNCT
eurjchem-365	256	11	the	the	DET
eurjchem-365	256	12	authors	author	NOUN
eurjchem-365	256	13	obtained	obtain	VERB
eurjchem-365	256	14	the	the	DET
eurjchem-365	256	15	amide	amide	NOUN
eurjchem-365	256	16	(	(	PUNCT
eurjchem-365	256	17	9	9	NUM
eurjchem-365	256	18	)	)	PUNCT
eurjchem-365	256	19	,	,	PUNCT
eurjchem-365	256	20	which	which	PRON
eurjchem-365	256	21	upon	upon	SCONJ
eurjchem-365	256	22	treatment	treatment	NOUN
eurjchem-365	256	23	with	with	ADP
eurjchem-365	256	24	acetic	acetic	ADJ
eurjchem-365	256	25	anhydride	anhydride	NOUN
eurjchem-365	256	26	underwent	underwent	NOUN
eurjchem-365	256	27	cyclization	cyclization	NOUN
eurjchem-365	256	28	to	to	ADP
eurjchem-365	256	29	the	the	DET
eurjchem-365	256	30	benzoxazinone	benzoxazinone	NOUN
eurjchem-365	256	31	derivative	derivative	NOUN
eurjchem-365	256	32	(	(	PUNCT
eurjchem-365	256	33	10	10	NUM
eurjchem-365	256	34	)	)	PUNCT
eurjchem-365	256	35	that	that	SCONJ
eurjchem-365	256	36	upon	upon	SCONJ
eurjchem-365	256	37	heating	heat	VERB
eurjchem-365	256	38	with	with	ADP
eurjchem-365	256	39	ammonium	ammonium	NOUN
eurjchem-365	256	40	acetate	acetate	NOUN
eurjchem-365	256	41	at	at	ADP
eurjchem-365	256	42	140‐160	140‐160	PROPN
eurjchem-365	256	43	oc	oc	NOUN
eurjchem-365	256	44	without	without	ADP
eurjchem-365	256	45	solvent	solvent	NOUN
eurjchem-365	256	46	afforded	afford	VERB
eurjchem-365	256	47	the	the	DET
eurjchem-365	256	48	corresponding	correspond	VERB
eurjchem-365	256	49	quinazolinone	quinazolinone	PROPN
eurjchem-365	256	50	derivative	derivative	NOUN
eurjchem-365	256	51	(	(	PUNCT
eurjchem-365	256	52	11	11	NUM
eurjchem-365	256	53	)	)	PUNCT
eurjchem-365	256	54	(	(	PUNCT
eurjchem-365	256	55	scheme	scheme	NOUN
eurjchem-365	256	56	1	1	NUM
eurjchem-365	256	57	)	)	PUNCT
eurjchem-365	256	58	.	.	PUNCT
eurjchem-365	257	1	on	on	ADP
eurjchem-365	257	2	the	the	DET
eurjchem-365	257	3	other	other	ADJ
eurjchem-365	257	4	hand	hand	NOUN
eurjchem-365	257	5	,	,	PUNCT
eurjchem-365	257	6	in	in	ADP
eurjchem-365	257	7	presence	presence	NOUN
eurjchem-365	257	8	of	of	ADP
eurjchem-365	257	9	pyridine	pyridine	NOUN
eurjchem-365	257	10	at	at	ADP
eurjchem-365	257	11	refluxing	refluxing	NOUN
eurjchem-365	257	12	temperature	temperature	NOUN
eurjchem-365	257	13	,	,	PUNCT
eurjchem-365	257	14	a	a	DET
eurjchem-365	257	15	mixture	mixture	NOUN
eurjchem-365	257	16	of	of	ADP
eurjchem-365	257	17	quinazolinone	quinazolinone	PROPN
eurjchem-365	257	18	derivative	derivative	NOUN
eurjchem-365	257	19	(	(	PUNCT
eurjchem-365	257	20	12	12	NUM
eurjchem-365	257	21	)	)	PUNCT
eurjchem-365	257	22	and	and	CCONJ
eurjchem-365	257	23	benzamide	benzamide	VERB
eurjchem-365	257	24	derivative	derivative	NOUN
eurjchem-365	257	25	(	(	PUNCT
eurjchem-365	257	26	13	13	NUM
eurjchem-365	257	27	)	)	PUNCT
eurjchem-365	257	28	was	be	AUX
eurjchem-365	257	29	obtained	obtain	VERB
eurjchem-365	257	30	.	.	PUNCT
eurjchem-365	258	1	the	the	DET
eurjchem-365	258	2	reaction	reaction	NOUN
eurjchem-365	258	3	probably	probably	ADV
eurjchem-365	258	4	proceeded	proceed	VERB
eurjchem-365	258	5	via	via	ADP
eurjchem-365	258	6	the	the	DET
eurjchem-365	258	7	formation	formation	NOUN
eurjchem-365	258	8	of	of	ADP
eurjchem-365	258	9	benzoxazinone	benzoxazinone	NOUN
eurjchem-365	258	10	(	(	PUNCT
eurjchem-365	258	11	10	10	NUM
eurjchem-365	258	12	)	)	PUNCT
eurjchem-365	258	13	followed	follow	VERB
eurjchem-365	258	14	by	by	ADP
eurjchem-365	258	15	further	further	ADJ
eurjchem-365	258	16	addition	addition	NOUN
eurjchem-365	258	17	of	of	ADP
eurjchem-365	258	18	anthranilic	anthranilic	ADJ
eurjchem-365	258	19	acid	acid	NOUN
eurjchem-365	258	20	molecule	molecule	NOUN
eurjchem-365	258	21	to	to	PART
eurjchem-365	258	22	give	give	VERB
eurjchem-365	258	23	(	(	PUNCT
eurjchem-365	258	24	13	13	NUM
eurjchem-365	258	25	)	)	PUNCT
eurjchem-365	258	26	which	which	PRON
eurjchem-365	258	27	underwent	undergo	VERB
eurjchem-365	258	28	cyclization	cyclization	NOUN
eurjchem-365	258	29	under	under	ADP
eurjchem-365	258	30	the	the	DET
eurjchem-365	258	31	reaction	reaction	NOUN
eurjchem-365	258	32	conditions	condition	NOUN
eurjchem-365	258	33	to	to	PART
eurjchem-365	258	34	afford	afford	VERB
eurjchem-365	258	35	the	the	DET
eurjchem-365	258	36	quinazolinone	quinazolinone	NOUN
eurjchem-365	258	37	(	(	PUNCT
eurjchem-365	258	38	12	12	NUM
eurjchem-365	258	39	)	)	PUNCT
eurjchem-365	258	40	(	(	PUNCT
eurjchem-365	258	41	scheme	scheme	NOUN
eurjchem-365	258	42	1	1	NUM
eurjchem-365	258	43	,	,	PUNCT
eurjchem-365	258	44	route	route	NOUN
eurjchem-365	258	45	a	a	PRON
eurjchem-365	258	46	)	)	PUNCT
eurjchem-365	258	47	.	.	PUNCT
eurjchem-365	259	1	204	204	NUM
eurjchem-365	259	2	shiba	shiba	NOUN
eurjchem-365	259	3	et	et	PROPN
eurjchem-365	259	4	al	al	PROPN
eurjchem-365	259	5	.	.	PUNCT
eurjchem-365	259	6	/	/	SYM
eurjchem-365	259	7	european	european	PROPN
eurjchem-365	259	8	journal	journal	PROPN
eurjchem-365	259	9	of	of	ADP
eurjchem-365	259	10	chemistry	chemistry	NOUN
eurjchem-365	259	11	2	2	NUM
eurjchem-365	259	12	(	(	PUNCT
eurjchem-365	259	13	2	2	NUM
eurjchem-365	259	14	)	)	PUNCT
eurjchem-365	259	15	(	(	PUNCT
eurjchem-365	259	16	2011	2011	NUM
eurjchem-365	259	17	)	)	PUNCT
eurjchem-365	259	18	200‐205	200‐205	NUM
eurjchem-365	259	19	scheme	scheme	NOUN
eurjchem-365	259	20	2	2	NUM
eurjchem-365	259	21	scheme	scheme	NOUN
eurjchem-365	259	22	3	3	NUM
eurjchem-365	259	23	the	the	DET
eurjchem-365	259	24	previous	previous	ADJ
eurjchem-365	259	25	pathway	pathway	NOUN
eurjchem-365	259	26	was	be	AUX
eurjchem-365	259	27	confirmed	confirm	VERB
eurjchem-365	259	28	by	by	ADP
eurjchem-365	259	29	reaction	reaction	NOUN
eurjchem-365	259	30	of	of	ADP
eurjchem-365	259	31	benzoxazinone	benzoxazinone	NOUN
eurjchem-365	259	32	(	(	PUNCT
eurjchem-365	259	33	10	10	NUM
eurjchem-365	259	34	)	)	PUNCT
eurjchem-365	259	35	with	with	ADP
eurjchem-365	259	36	anthranilic	anthranilic	ADJ
eurjchem-365	259	37	acid	acid	NOUN
eurjchem-365	259	38	in	in	ADP
eurjchem-365	259	39	ethanol	ethanol	NOUN
eurjchem-365	259	40	to	to	PART
eurjchem-365	259	41	yield	yield	VERB
eurjchem-365	259	42	a	a	DET
eurjchem-365	259	43	mixture	mixture	NOUN
eurjchem-365	259	44	of	of	ADP
eurjchem-365	259	45	12:13	12:13	NUM
eurjchem-365	259	46	in	in	ADP
eurjchem-365	259	47	10:90	10:90	NUM
eurjchem-365	259	48	%	%	NOUN
eurjchem-365	259	49	yield	yield	NOUN
eurjchem-365	259	50	,	,	PUNCT
eurjchem-365	259	51	respectively	respectively	ADV
eurjchem-365	259	52	,	,	PUNCT
eurjchem-365	259	53	while	while	SCONJ
eurjchem-365	259	54	upon	upon	SCONJ
eurjchem-365	259	55	heating	heating	NOUN
eurjchem-365	259	56	compound	compound	NOUN
eurjchem-365	259	57	10	10	NUM
eurjchem-365	259	58	with	with	ADP
eurjchem-365	259	59	anthranilic	anthranilic	ADJ
eurjchem-365	259	60	acid	acid	NOUN
eurjchem-365	259	61	at	at	ADP
eurjchem-365	259	62	140‐150	140‐150	NUM
eurjchem-365	259	63	oc	oc	NOUN
eurjchem-365	259	64	in	in	ADP
eurjchem-365	259	65	absence	absence	NOUN
eurjchem-365	259	66	of	of	ADP
eurjchem-365	259	67	solvent	solvent	NOUN
eurjchem-365	259	68	,	,	PUNCT
eurjchem-365	259	69	the	the	DET
eurjchem-365	259	70	mixture	mixture	NOUN
eurjchem-365	259	71	12:13	12:13	NUM
eurjchem-365	259	72	was	be	AUX
eurjchem-365	259	73	obtained	obtain	VERB
eurjchem-365	259	74	in	in	ADP
eurjchem-365	259	75	80:20	80:20	NUM
eurjchem-365	259	76	%	%	NOUN
eurjchem-365	259	77	yield	yield	NOUN
eurjchem-365	259	78	,	,	PUNCT
eurjchem-365	259	79	respectively	respectively	ADV
eurjchem-365	259	80	(	(	PUNCT
eurjchem-365	259	81	scheme	scheme	NOUN
eurjchem-365	259	82	1	1	NUM
eurjchem-365	259	83	)	)	PUNCT
eurjchem-365	259	84	.	.	PUNCT
eurjchem-365	260	1	furthermore	furthermore	ADV
eurjchem-365	260	2	,	,	PUNCT
eurjchem-365	260	3	refluxing	refluxing	NOUN
eurjchem-365	260	4	benzamide	benzamide	NOUN
eurjchem-365	260	5	derivative	derivative	NOUN
eurjchem-365	260	6	(	(	PUNCT
eurjchem-365	260	7	13	13	NUM
eurjchem-365	260	8	)	)	PUNCT
eurjchem-365	260	9	in	in	ADP
eurjchem-365	260	10	freshly	freshly	ADV
eurjchem-365	260	11	distilled	distil	VERB
eurjchem-365	260	12	acetic	acetic	ADJ
eurjchem-365	260	13	anhydride	anhydride	NOUN
eurjchem-365	260	14	yielded	yield	VERB
eurjchem-365	260	15	a	a	DET
eurjchem-365	260	16	mixture	mixture	NOUN
eurjchem-365	260	17	of	of	ADP
eurjchem-365	260	18	benzoxazinone	benzoxazinone	PROPN
eurjchem-365	260	19	derivative	derivative	NOUN
eurjchem-365	260	20	(	(	PUNCT
eurjchem-365	260	21	14	14	NUM
eurjchem-365	260	22	)	)	PUNCT
eurjchem-365	260	23	besides	besides	SCONJ
eurjchem-365	260	24	benzoxazinone	benzoxazinone	NOUN
eurjchem-365	260	25	(	(	PUNCT
eurjchem-365	260	26	10	10	NUM
eurjchem-365	260	27	)	)	PUNCT
eurjchem-365	260	28	and	and	CCONJ
eurjchem-365	260	29	quinazolinone	quinazolinone	NOUN
eurjchem-365	260	30	(	(	PUNCT
eurjchem-365	260	31	12	12	NUM
eurjchem-365	260	32	)	)	PUNCT
eurjchem-365	260	33	in	in	ADP
eurjchem-365	260	34	45:5:25	45:5:25	NUM
eurjchem-365	260	35	%	%	NOUN
eurjchem-365	260	36	yield	yield	NOUN
eurjchem-365	260	37	via	via	ADP
eurjchem-365	260	38	the	the	DET
eurjchem-365	260	39	available	available	ADJ
eurjchem-365	260	40	cyclization	cyclization	NOUN
eurjchem-365	260	41	in	in	ADP
eurjchem-365	260	42	route	route	NOUN
eurjchem-365	260	43	(	(	PUNCT
eurjchem-365	260	44	a	a	NOUN
eurjchem-365	260	45	)	)	PUNCT
eurjchem-365	260	46	or	or	CCONJ
eurjchem-365	260	47	(	(	PUNCT
eurjchem-365	260	48	b	b	NOUN
eurjchem-365	260	49	)	)	PUNCT
eurjchem-365	260	50	to	to	PART
eurjchem-365	260	51	give	give	VERB
eurjchem-365	260	52	12	12	NUM
eurjchem-365	260	53	and	and	CCONJ
eurjchem-365	260	54	14	14	NUM
eurjchem-365	260	55	and/or	and/or	CCONJ
eurjchem-365	260	56	unexpected	unexpected	ADJ
eurjchem-365	260	57	addition	addition	NOUN
eurjchem-365	260	58	via	via	ADP
eurjchem-365	260	59	route	route	NOUN
eurjchem-365	260	60	(	(	PUNCT
eurjchem-365	260	61	a	a	NOUN
eurjchem-365	260	62	)	)	PUNCT
eurjchem-365	260	63	with	with	ADP
eurjchem-365	260	64	subsequent	subsequent	ADJ
eurjchem-365	260	65	cleavage	cleavage	NOUN
eurjchem-365	260	66	of	of	ADP
eurjchem-365	260	67	anthranilic	anthranilic	ADJ
eurjchem-365	260	68	acid	acid	NOUN
eurjchem-365	260	69	moiety	moiety	NOUN
eurjchem-365	260	70	to	to	PART
eurjchem-365	260	71	give	give	VERB
eurjchem-365	260	72	10	10	NUM
eurjchem-365	260	73	(	(	PUNCT
eurjchem-365	260	74	scheme	scheme	NOUN
eurjchem-365	260	75	1	1	NUM
eurjchem-365	260	76	)	)	PUNCT
eurjchem-365	260	77	.	.	PUNCT
eurjchem-365	261	1	hydrazinolysis	hydrazinolysis	NOUN
eurjchem-365	261	2	of	of	ADP
eurjchem-365	261	3	benzoxazinone	benzoxazinone	NOUN
eurjchem-365	261	4	(	(	PUNCT
eurjchem-365	261	5	10	10	NUM
eurjchem-365	261	6	)	)	PUNCT
eurjchem-365	261	7	with	with	ADP
eurjchem-365	261	8	hydrazine	hydrazine	NOUN
eurjchem-365	261	9	hydrate	hydrate	NOUN
eurjchem-365	261	10	in	in	ADP
eurjchem-365	261	11	refluxing	refluxing	NOUN
eurjchem-365	261	12	ethanol	ethanol	NOUN
eurjchem-365	261	13	afforded	afford	VERB
eurjchem-365	261	14	the	the	DET
eurjchem-365	261	15	hydrazide	hydrazide	ADJ
eurjchem-365	261	16	derivative	derivative	ADJ
eurjchem-365	261	17	15	15	NUM
eurjchem-365	261	18	(	(	PUNCT
eurjchem-365	261	19	scheme	scheme	NOUN
eurjchem-365	261	20	1	1	NUM
eurjchem-365	261	21	)	)	PUNCT
eurjchem-365	261	22	,	,	PUNCT
eurjchem-365	261	23	which	which	PRON
eurjchem-365	261	24	probably	probably	ADV
eurjchem-365	261	25	produced	produce	VERB
eurjchem-365	261	26	according	accord	VERB
eurjchem-365	261	27	to	to	ADP
eurjchem-365	261	28	the	the	DET
eurjchem-365	261	29	plausible	plausible	ADJ
eurjchem-365	261	30	mechanism	mechanism	NOUN
eurjchem-365	261	31	shown	show	VERB
eurjchem-365	261	32	in	in	ADP
eurjchem-365	261	33	scheme	scheme	NOUN
eurjchem-365	261	34	2	2	NUM
eurjchem-365	261	35	.	.	PUNCT
eurjchem-365	261	36	with	with	ADP
eurjchem-365	261	37	2‐aminopyridine	2‐aminopyridine	NUM
eurjchem-365	261	38	,	,	PUNCT
eurjchem-365	261	39	acid	acid	ADJ
eurjchem-365	261	40	chloride	chloride	NOUN
eurjchem-365	261	41	(	(	PUNCT
eurjchem-365	261	42	1	1	NUM
eurjchem-365	261	43	)	)	PUNCT
eurjchem-365	261	44	gave	give	VERB
eurjchem-365	261	45	the	the	DET
eurjchem-365	261	46	fused	fuse	VERB
eurjchem-365	261	47	bicyclic	bicyclic	NOUN
eurjchem-365	261	48	system	system	NOUN
eurjchem-365	261	49	pyrido[1,2‐a	pyrido[1,2‐a	NOUN
eurjchem-365	261	50	]	]	PUNCT
eurjchem-365	261	51	pyrimidine	pyrimidine	NOUN
eurjchem-365	261	52	derivative	derivative	NOUN
eurjchem-365	261	53	(	(	PUNCT
eurjchem-365	261	54	16	16	NUM
eurjchem-365	261	55	)	)	PUNCT
eurjchem-365	261	56	(	(	PUNCT
eurjchem-365	261	57	scheme	scheme	NOUN
eurjchem-365	261	58	1	1	NUM
eurjchem-365	261	59	)	)	PUNCT
eurjchem-365	261	60	.	.	PUNCT
eurjchem-365	262	1	the	the	DET
eurjchem-365	262	2	formation	formation	NOUN
eurjchem-365	262	3	of	of	ADP
eurjchem-365	262	4	pyridopyrimidine	pyridopyrimidine	NOUN
eurjchem-365	262	5	16	16	NUM
eurjchem-365	262	6	can	can	AUX
eurjchem-365	262	7	be	be	AUX
eurjchem-365	262	8	interpreted	interpret	VERB
eurjchem-365	262	9	as	as	ADP
eurjchem-365	262	10	shown	show	VERB
eurjchem-365	262	11	in	in	ADP
eurjchem-365	262	12	(	(	PUNCT
eurjchem-365	262	13	scheme	scheme	NOUN
eurjchem-365	262	14	3	3	NUM
eurjchem-365	262	15	)	)	PUNCT
eurjchem-365	262	16	through	through	ADP
eurjchem-365	262	17	normal	normal	ADJ
eurjchem-365	262	18	substitution	substitution	NOUN
eurjchem-365	262	19	by	by	ADP
eurjchem-365	262	20	tetrahedral	tetrahedral	ADJ
eurjchem-365	262	21	mechanism	mechanism	NOUN
eurjchem-365	262	22	on	on	ADP
eurjchem-365	262	23	the	the	DET
eurjchem-365	262	24	carbonyl	carbonyl	NOUN
eurjchem-365	262	25	functionality	functionality	NOUN
eurjchem-365	262	26	of	of	ADP
eurjchem-365	262	27	compound	compound	NOUN
eurjchem-365	262	28	1	1	NUM
eurjchem-365	262	29	followed	follow	VERB
eurjchem-365	262	30	by	by	ADP
eurjchem-365	262	31	1,3‐proton	1,3‐proton	NUM
eurjchem-365	262	32	shift	shift	NOUN
eurjchem-365	262	33	and	and	CCONJ
eurjchem-365	262	34	addition	addition	NOUN
eurjchem-365	262	35	to	to	ADP
eurjchem-365	262	36	‐unsaturated	‐unsaturate	VERB
eurjchem-365	262	37	nitrile	nitrile	ADV
eurjchem-365	262	38	with	with	ADP
eurjchem-365	262	39	subsequent	subsequent	ADJ
eurjchem-365	262	40	dehydrogenation	dehydrogenation	NOUN
eurjchem-365	262	41	[	[	X
eurjchem-365	262	42	24	24	NUM
eurjchem-365	262	43	]	]	PUNCT
eurjchem-365	262	44	under	under	ADP
eurjchem-365	262	45	the	the	DET
eurjchem-365	262	46	reaction	reaction	NOUN
eurjchem-365	262	47	conditions	condition	NOUN
eurjchem-365	262	48	,	,	PUNCT
eurjchem-365	262	49	according	accord	VERB
eurjchem-365	262	50	to	to	ADP
eurjchem-365	262	51	the	the	DET
eurjchem-365	262	52	pathway	pathway	NOUN
eurjchem-365	262	53	shown	show	VERB
eurjchem-365	262	54	in	in	ADP
eurjchem-365	262	55	scheme	scheme	NOUN
eurjchem-365	262	56	3	3	NUM
eurjchem-365	262	57	.	.	PUNCT
eurjchem-365	263	1	reaction	reaction	NOUN
eurjchem-365	263	2	of	of	ADP
eurjchem-365	263	3	chloride	chloride	NOUN
eurjchem-365	263	4	(	(	PUNCT
eurjchem-365	263	5	1	1	NUM
eurjchem-365	263	6	)	)	PUNCT
eurjchem-365	263	7	with	with	ADP
eurjchem-365	263	8	2‐aminothiophenol	2‐aminothiophenol	PROPN
eurjchem-365	263	9	gave	give	VERB
eurjchem-365	263	10	the	the	DET
eurjchem-365	263	11	benzo‐1,5‐thiazepinone	benzo‐1,5‐thiazepinone	ADJ
eurjchem-365	263	12	derivative	derivative	NOUN
eurjchem-365	263	13	(	(	PUNCT
eurjchem-365	263	14	17	17	NUM
eurjchem-365	263	15	)	)	PUNCT
eurjchem-365	263	16	(	(	PUNCT
eurjchem-365	263	17	scheme	scheme	NOUN
eurjchem-365	263	18	1	1	NUM
eurjchem-365	263	19	)	)	PUNCT
eurjchem-365	263	20	whereas	whereas	SCONJ
eurjchem-365	263	21	the	the	DET
eurjchem-365	263	22	treatment	treatment	NOUN
eurjchem-365	263	23	of	of	ADP
eurjchem-365	263	24	1	1	NUM
eurjchem-365	263	25	with	with	ADP
eurjchem-365	263	26	benzoylhydrazine	benzoylhydrazine	NOUN
eurjchem-365	263	27	afforded	afford	VERB
eurjchem-365	263	28	the	the	DET
eurjchem-365	263	29	corresponding	correspond	VERB
eurjchem-365	263	30	hydrazide	hydrazide	ADJ
eurjchem-365	263	31	derivative	derivative	NOUN
eurjchem-365	263	32	(	(	PUNCT
eurjchem-365	263	33	18	18	NUM
eurjchem-365	263	34	)	)	PUNCT
eurjchem-365	263	35	which	which	PRON
eurjchem-365	263	36	on	on	ADP
eurjchem-365	263	37	heating	heat	VERB
eurjchem-365	263	38	with	with	ADP
eurjchem-365	263	39	pocl3	pocl3	NOUN
eurjchem-365	263	40	gave	give	VERB
eurjchem-365	263	41	the	the	DET
eurjchem-365	263	42	oxadiazole	oxadiazole	NOUN
eurjchem-365	263	43	derivative	derivative	NOUN
eurjchem-365	263	44	19	19	NUM
eurjchem-365	263	45	.	.	PUNCT
eurjchem-365	264	1	with	with	ADP
eurjchem-365	264	2	2‐aminophenol	2‐aminophenol	NUM
eurjchem-365	264	3	,	,	PUNCT
eurjchem-365	264	4	the	the	DET
eurjchem-365	264	5	isolated	isolated	ADJ
eurjchem-365	264	6	product	product	NOUN
eurjchem-365	264	7	was	be	AUX
eurjchem-365	264	8	the	the	DET
eurjchem-365	264	9	amide	amide	NOUN
eurjchem-365	264	10	derivative	derivative	NOUN
eurjchem-365	264	11	(	(	PUNCT
eurjchem-365	264	12	20	20	NUM
eurjchem-365	264	13	)	)	PUNCT
eurjchem-365	264	14	which	which	PRON
eurjchem-365	264	15	was	be	AUX
eurjchem-365	264	16	dehydrated	dehydrate	VERB
eurjchem-365	264	17	under	under	ADP
eurjchem-365	264	18	the	the	DET
eurjchem-365	264	19	effect	effect	NOUN
eurjchem-365	264	20	of	of	ADP
eurjchem-365	264	21	pocl3	pocl3	NOUN
eurjchem-365	264	22	to	to	PART
eurjchem-365	264	23	give	give	VERB
eurjchem-365	264	24	the	the	DET
eurjchem-365	264	25	benzoxazole	benzoxazole	NOUN
eurjchem-365	264	26	derivative	derivative	NOUN
eurjchem-365	264	27	.	.	PUNCT
eurjchem-365	265	1	4	4	X
eurjchem-365	265	2	.	.	X
eurjchem-365	265	3	conclusion	conclusion	NOUN
eurjchem-365	265	4	(	(	PUNCT
eurjchem-365	265	5	e)2‐cyano‐3‐phenyl‐2‐propenoyl	e)2‐cyano‐3‐phenyl‐2‐propenoyl	PROPN
eurjchem-365	265	6	chloride	chloride	NOUN
eurjchem-365	265	7	could	could	AUX
eurjchem-365	265	8	be	be	AUX
eurjchem-365	265	9	utilized	utilize	VERB
eurjchem-365	265	10	in	in	ADP
eurjchem-365	265	11	the	the	DET
eurjchem-365	265	12	synthesis	synthesis	NOUN
eurjchem-365	265	13	of	of	ADP
eurjchem-365	265	14	some	some	DET
eurjchem-365	265	15	heterocyclic	heterocyclic	ADJ
eurjchem-365	265	16	systems	system	NOUN
eurjchem-365	265	17	like	like	ADP
eurjchem-365	265	18	benzoxazinone	benzoxazinone	PROPN
eurjchem-365	265	19	,	,	PUNCT
eurjchem-365	265	20	quinazolinone	quinazolinone	NUM
eurjchem-365	265	21	,	,	PUNCT
eurjchem-365	265	22	pyridopyrimidine	pyridopyrimidine	NOUN
eurjchem-365	265	23	,	,	PUNCT
eurjchem-365	265	24	benzothi‐	benzothi‐	NOUN
eurjchem-365	265	25	azepine	azepine	PROPN
eurjchem-365	265	26	,	,	PUNCT
eurjchem-365	265	27	oxadiazole	oxadiazole	NOUN
eurjchem-365	265	28	and	and	CCONJ
eurjchem-365	265	29	benzoxazole	benzoxazole	NOUN
eurjchem-365	265	30	via	via	ADP
eurjchem-365	265	31	2‐propenoylamides	2‐propenoylamide	NOUN
eurjchem-365	265	32	as	as	ADP
eurjchem-365	265	33	intermediates	intermediate	NOUN
eurjchem-365	265	34	.	.	PUNCT
eurjchem-365	266	1	acknowledgement	acknowledgement	PROPN
eurjchem-365	266	2	technical	technical	ADJ
eurjchem-365	266	3	support	support	NOUN
eurjchem-365	266	4	from	from	ADP
eurjchem-365	266	5	department	department	NOUN
eurjchem-365	266	6	of	of	ADP
eurjchem-365	266	7	chemistry	chemistry	NOUN
eurjchem-365	266	8	,	,	PUNCT
eurjchem-365	266	9	faculty	faculty	NOUN
eurjchem-365	266	10	of	of	ADP
eurjchem-365	266	11	science	science	NOUN
eurjchem-365	266	12	,	,	PUNCT
eurjchem-365	266	13	ain	ain	PROPN
eurjchem-365	266	14	shams	sham	NOUN
eurjchem-365	266	15	university	university	PROPN
eurjchem-365	266	16	is	be	AUX
eurjchem-365	266	17	gratefully	gratefully	ADV
eurjchem-365	266	18	acknowledged	acknowledge	VERB
eurjchem-365	266	19	.	.	PUNCT
eurjchem-365	267	1	references	reference	NOUN
eurjchem-365	267	2	[	[	X
eurjchem-365	267	3	1	1	NUM
eurjchem-365	267	4	]	]	PUNCT
eurjchem-365	267	5	.	.	PUNCT
eurjchem-365	268	1	li	li	PROPN
eurjchem-365	268	2	,	,	PUNCT
eurjchem-365	268	3	y.	y.	PROPN
eurjchem-365	268	4	l.	l.	PROPN
eurjchem-365	268	5	;	;	PUNCT
eurjchem-365	268	6	xu	xu	PROPN
eurjchem-365	268	7	,	,	PUNCT
eurjchem-365	268	8	w.	w.	PROPN
eurjchem-365	268	9	f.	f.	PROPN
eurjchem-365	268	10	bioorgan	bioorgan	PROPN
eurjchem-365	268	11	.	.	PUNCT
eurjchem-365	269	1	med	med	PROPN
eurjchem-365	269	2	.	.	PROPN
eurjchem-365	269	3	chem	chem	PROPN
eurjchem-365	269	4	.	.	PUNCT
eurjchem-365	270	1	2004	2004	NUM
eurjchem-365	270	2	,	,	PUNCT
eurjchem-365	270	3	12(19	12(19	NUM
eurjchem-365	270	4	)	)	PUNCT
eurjchem-365	270	5	,	,	PUNCT
eurjchem-365	270	6	5171‐5180	5171‐5180	NUM
eurjchem-365	270	7	.	.	PUNCT
eurjchem-365	271	1	[	[	X
eurjchem-365	271	2	2	2	NUM
eurjchem-365	271	3	]	]	PUNCT
eurjchem-365	271	4	.	.	PUNCT
eurjchem-365	272	1	sousa	sousa	PROPN
eurjchem-365	272	2	,	,	PUNCT
eurjchem-365	272	3	j.	j.	PROPN
eurjchem-365	272	4	b.	b.	PROPN
eurjchem-365	272	5	;	;	PUNCT
eurjchem-365	272	6	calheiros	calheiros	PROPN
eurjchem-365	272	7	,	,	PUNCT
eurjchem-365	272	8	r.	r.	PROPN
eurjchem-365	272	9	;	;	PUNCT
eurjchem-365	272	10	rio	rio	PROPN
eurjchem-365	272	11	,	,	PUNCT
eurjchem-365	272	12	v.	v.	PROPN
eurjchem-365	272	13	;	;	PUNCT
eurjchem-365	272	14	borges	borge	NOUN
eurjchem-365	272	15	,	,	PUNCT
eurjchem-365	272	16	f.	f.	PROPN
eurjchem-365	272	17	;	;	PUNCT
eurjchem-365	272	18	marques	marques	PROPN
eurjchem-365	272	19	,	,	PUNCT
eurjchem-365	272	20	m.	m.	NOUN
eurjchem-365	272	21	p.	p.	PROPN
eurjchem-365	272	22	m.	m.	NOUN
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eurjchem-365	339	8	;	;	PUNCT
eurjchem-365	339	9	danion‐bougot	danion‐bougot	PROPN
eurjchem-365	339	10	,	,	PUNCT
eurjchem-365	339	11	r.	r.	PROPN
eurjchem-365	339	12	;	;	PUNCT
eurjchem-365	339	13	danion	danion	NOUN
eurjchem-365	339	14	,	,	PUNCT
eurjchem-365	339	15	d.	d.	PROPN
eurjchem-365	339	16	synthesis	synthesis	PROPN
eurjchem-365	339	17	1994	1994	NUM
eurjchem-365	339	18	,	,	PUNCT
eurjchem-365	339	19	1	1	NUM
eurjchem-365	339	20	,	,	PUNCT
eurjchem-365	339	21	56‐60	56‐60	NUM
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eurjchem-365	340	1	[	[	X
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eurjchem-365	340	3	]	]	PUNCT
eurjchem-365	340	4	.	.	PUNCT
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eurjchem-365	341	2	,	,	PUNCT
eurjchem-365	341	3	t.	t.	PROPN
eurjchem-365	341	4	c.	c.	PROPN
eurjchem-365	341	5	;	;	PUNCT
eurjchem-365	341	6	chen	chen	PROPN
eurjchem-365	341	7	,	,	PUNCT
eurjchem-365	341	8	y.	y.	PROPN
eurjchem-365	341	9	l.	l.	PROPN
eurjchem-365	341	10	;	;	PUNCT
eurjchem-365	341	11	lee	lee	PROPN
eurjchem-365	341	12	,	,	PUNCT
eurjchem-365	341	13	k.	k.	PROPN
eurjchem-365	341	14	h.	h.	PROPN
eurjchem-365	341	15	;	;	PUNCT
eurjchem-365	341	16	tzeng	tzeng	PROPN
eurjchem-365	341	17	,	,	PUNCT
eurjchem-365	341	18	c.	c.	PROPN
eurjchem-365	341	19	c.	c.	PROPN
eurjchem-365	341	20	tetrahedron	tetrahedron	PROPN
eurjchem-365	341	21	lett	lett	PROPN
eurjchem-365	341	22	.	.	PUNCT
eurjchem-365	341	23	1996	1996	NUM
eurjchem-365	341	24	,	,	PUNCT
eurjchem-365	341	25	37(35	37(35	NUM
eurjchem-365	341	26	)	)	PUNCT
eurjchem-365	341	27	,	,	PUNCT
eurjchem-365	341	28	6369‐6370	6369‐6370	NUM
eurjchem-365	341	29	.	.	PUNCT
eurjchem-365	342	1	[	[	X
eurjchem-365	342	2	24	24	NUM
eurjchem-365	342	3	]	]	PUNCT
eurjchem-365	342	4	.	.	PUNCT
eurjchem-365	343	1	march	march	PROPN
eurjchem-365	343	2	,	,	PUNCT
eurjchem-365	343	3	j.	j.	PROPN
eurjchem-365	343	4	advanced	advance	VERB
eurjchem-365	343	5	organic	organic	ADJ
eurjchem-365	343	6	chemistry	chemistry	NOUN
eurjchem-365	343	7	,	,	PUNCT
eurjchem-365	343	8	3rd	3rd	ADJ
eurjchem-365	343	9	edition	edition	NOUN
eurjchem-365	343	10	,	,	PUNCT
eurjchem-365	343	11	john	john	PROPN
eurjchem-365	343	12	wiley	wiley	PROPN
eurjchem-365	343	13	&	&	CCONJ
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eurjchem-365	343	15	.	.	PUNCT
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eurjchem-365	344	2	pub	pub	NOUN
eurjchem-365	344	3	.	.	PUNCT
eurjchem-365	345	1	,	,	PUNCT
eurjchem-365	345	2	new	new	PROPN
eurjchem-365	345	3	york	york	PROPN
eurjchem-365	345	4	p	p	PROPN
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eurjchem-365	345	6	,	,	PUNCT
eurjchem-365	345	7	1985	1985	NUM
eurjchem-365	345	8	.	.	PUNCT