id	sid	tid	token	lemma	pos
eurjchem-376	1	1	untitled	untitle	VERB
eurjchem-376	1	2	european	european	PROPN
eurjchem-376	1	3	journal	journal	PROPN
eurjchem-376	1	4	of	of	ADP
eurjchem-376	1	5	chemistry	chemistry	NOUN
eurjchem-376	1	6	2	2	NUM
eurjchem-376	1	7	(	(	PUNCT
eurjchem-376	1	8	3	3	NUM
eurjchem-376	1	9	)	)	PUNCT
eurjchem-376	1	10	(	(	PUNCT
eurjchem-376	1	11	2011	2011	NUM
eurjchem-376	1	12	)	)	PUNCT
eurjchem-376	1	13	295‐299	295‐299	PROPN
eurjchem-376	1	14	european	european	PROPN
eurjchem-376	1	15	journal	journal	PROPN
eurjchem-376	1	16	of	of	ADP
eurjchem-376	1	17	chemistry	chemistry	NOUN
eurjchem-376	1	18	issn	issn	PROPN
eurjchem-376	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-376	1	20	(	(	PUNCT
eurjchem-376	1	21	print	print	NOUN
eurjchem-376	1	22	)	)	PUNCT
eurjchem-376	1	23	/	/	SYM
eurjchem-376	1	24	issn	issn	PROPN
eurjchem-376	1	25	2153‐2257	2153‐2257	NUM
eurjchem-376	1	26	(	(	PUNCT
eurjchem-376	1	27	online	online	ADJ
eurjchem-376	1	28	)	)	PUNCT
eurjchem-376	1	29			NOUN
eurjchem-376	1	30	2011	2011	NUM
eurjchem-376	1	31	eurjchem	eurjchem	PROPN
eurjchem-376	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-376	1	33	/	/	SYM
eurjchem-376	1	34	eurjchem.2.3.295‐299.376	eurjchem.2.3.295‐299.376	PROPN
eurjchem-376	1	35	european	european	PROPN
eurjchem-376	1	36	journal	journal	PROPN
eurjchem-376	1	37	of	of	ADP
eurjchem-376	1	38	chemistry	chemistry	PROPN
eurjchem-376	1	39	journal	journal	PROPN
eurjchem-376	1	40	homepage	homepage	NOUN
eurjchem-376	1	41	:	:	PUNCT
eurjchem-376	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-376	1	43	synthesis	synthesis	NOUN
eurjchem-376	1	44	of	of	ADP
eurjchem-376	1	45	nitrogen	nitrogen	NOUN
eurjchem-376	1	46	heterocycles	heterocycle	NOUN
eurjchem-376	1	47	from	from	ADP
eurjchem-376	1	48	ethyl	ethyl	PROPN
eurjchem-376	1	49	3‐(6‐dibenzothiophen‐2‐yl‐pyridazin‐3‐ylamino)‐3‐oxopropanoate	3‐(6‐dibenzothiophen‐2‐yl‐pyridazin‐3‐ylamino)‐3‐oxopropanoate	NUM
eurjchem-376	1	50	mohamed	mohamed	PROPN
eurjchem-376	1	51	sayed	sayed	PROPN
eurjchem-376	1	52	behalo	behalo	PROPN
eurjchem-376	1	53	*	*	PROPN
eurjchem-376	1	54	and	and	CCONJ
eurjchem-376	1	55	aly	aly	PROPN
eurjchem-376	1	56	abdelmaboud	abdelmaboud	PROPN
eurjchem-376	1	57	aly	aly	PROPN
eurjchem-376	1	58	department	department	PROPN
eurjchem-376	1	59	of	of	ADP
eurjchem-376	1	60	chemistry	chemistry	NOUN
eurjchem-376	1	61	,	,	PUNCT
eurjchem-376	1	62	faculty	faculty	NOUN
eurjchem-376	1	63	of	of	ADP
eurjchem-376	1	64	science	science	NOUN
eurjchem-376	1	65	,	,	PUNCT
eurjchem-376	1	66	benha	benha	VERB
eurjchem-376	1	67	university	university	NOUN
eurjchem-376	1	68	,	,	PUNCT
eurjchem-376	1	69	benha	benha	NOUN
eurjchem-376	1	70	,	,	PUNCT
eurjchem-376	1	71	13518	13518	NUM
eurjchem-376	1	72	,	,	PUNCT
eurjchem-376	1	73	egypt	egypt	PROPN
eurjchem-376	1	74	*	*	PUNCT
eurjchem-376	1	75	corresponding	correspond	VERB
eurjchem-376	1	76	author	author	NOUN
eurjchem-376	1	77	at	at	ADP
eurjchem-376	1	78	:	:	PUNCT
eurjchem-376	1	79	department	department	NOUN
eurjchem-376	1	80	of	of	ADP
eurjchem-376	1	81	chemistry	chemistry	NOUN
eurjchem-376	1	82	,	,	PUNCT
eurjchem-376	1	83	faculty	faculty	NOUN
eurjchem-376	1	84	of	of	ADP
eurjchem-376	1	85	science	science	NOUN
eurjchem-376	1	86	,	,	PUNCT
eurjchem-376	1	87	benha	benha	VERB
eurjchem-376	1	88	university	university	NOUN
eurjchem-376	1	89	,	,	PUNCT
eurjchem-376	1	90	benha	benha	NOUN
eurjchem-376	1	91	,	,	PUNCT
eurjchem-376	1	92	13518	13518	NUM
eurjchem-376	1	93	,	,	PUNCT
eurjchem-376	1	94	egypt	egypt	PROPN
eurjchem-376	1	95	.	.	PUNCT
eurjchem-376	2	1	tel	tel	PROPN
eurjchem-376	2	2	.	.	PROPN
eurjchem-376	2	3	:	:	PUNCT
eurjchem-376	3	1	+20101599607	+20101599607	ADJ
eurjchem-376	3	2	;	;	PUNCT
eurjchem-376	3	3	fax	fax	NOUN
eurjchem-376	3	4	:	:	PUNCT
eurjchem-376	3	5	+20133222578	+20133222578	PROPN
eurjchem-376	3	6	.	.	PUNCT
eurjchem-376	3	7	e‐mail	e‐mail	PUNCT
eurjchem-376	4	1	address	address	NOUN
eurjchem-376	4	2	:	:	PUNCT
eurjchem-376	4	3	mohamedbehalo@hotmail.com	mohamedbehalo@hotmail.com	X
eurjchem-376	4	4	(	(	PUNCT
eurjchem-376	4	5	m.s	m.s	PROPN
eurjchem-376	4	6	.	.	PROPN
eurjchem-376	4	7	behalo	behalo	PROPN
eurjchem-376	4	8	)	)	PUNCT
eurjchem-376	4	9	.	.	PUNCT
eurjchem-376	5	1	article	article	NOUN
eurjchem-376	5	2	information	information	PROPN
eurjchem-376	5	3	abstract	abstract	ADV
eurjchem-376	5	4	received	receive	VERB
eurjchem-376	5	5	:	:	PUNCT
eurjchem-376	5	6	23	23	NUM
eurjchem-376	5	7	december	december	PROPN
eurjchem-376	5	8	2010	2010	NUM
eurjchem-376	5	9	received	receive	VERB
eurjchem-376	5	10	in	in	ADP
eurjchem-376	5	11	revised	revise	VERB
eurjchem-376	5	12	form	form	NOUN
eurjchem-376	5	13	:	:	PUNCT
eurjchem-376	5	14	28	28	NUM
eurjchem-376	5	15	march	march	NOUN
eurjchem-376	5	16	2011	2011	NUM
eurjchem-376	5	17	accepted	accept	VERB
eurjchem-376	5	18	:	:	PUNCT
eurjchem-376	5	19	29	29	NUM
eurjchem-376	5	20	march	march	PROPN
eurjchem-376	5	21	2011	2011	NUM
eurjchem-376	5	22	online	online	NOUN
eurjchem-376	5	23	:	:	PUNCT
eurjchem-376	5	24	30	30	NUM
eurjchem-376	5	25	september	september	PROPN
eurjchem-376	5	26	2011	2011	NUM
eurjchem-376	5	27	keywords	keyword	VERB
eurjchem-376	5	28	an	an	DET
eurjchem-376	5	29	efficient	efficient	ADJ
eurjchem-376	5	30	synthesis	synthesis	NOUN
eurjchem-376	5	31	of	of	ADP
eurjchem-376	5	32	nitrogen‐containing	nitrogen‐containe	VERB
eurjchem-376	5	33	heterocycles	heterocycle	NOUN
eurjchem-376	5	34	pyrazole	pyrazole	NOUN
eurjchem-376	5	35	,	,	PUNCT
eurjchem-376	5	36	triazole	triazole	NOUN
eurjchem-376	5	37	,	,	PUNCT
eurjchem-376	5	38	pyridinone	pyridinone	NOUN
eurjchem-376	5	39	and	and	CCONJ
eurjchem-376	5	40	pyrimidinone	pyrimidinone	ADJ
eurjchem-376	5	41	derivatives	derivative	NOUN
eurjchem-376	5	42	from	from	ADP
eurjchem-376	5	43	ethyl	ethyl	PROPN
eurjchem-376	5	44	3‐(6‐dibenzothiophen‐2‐yl‐pyridazin‐3‐ylamino)‐3‐	3‐(6‐dibenzothiophen‐2‐yl‐pyridazin‐3‐ylamino)‐3‐	NUM
eurjchem-376	5	45	oxopropanoate	oxopropanoate	NOUN
eurjchem-376	5	46	(	(	PUNCT
eurjchem-376	5	47	2	2	X
eurjchem-376	5	48	)	)	PUNCT
eurjchem-376	5	49	was	be	AUX
eurjchem-376	5	50	described	describe	VERB
eurjchem-376	5	51	.	.	PUNCT
eurjchem-376	6	1	the	the	DET
eurjchem-376	6	2	structures	structure	NOUN
eurjchem-376	6	3	of	of	ADP
eurjchem-376	6	4	all	all	DET
eurjchem-376	6	5	products	product	NOUN
eurjchem-376	6	6	were	be	AUX
eurjchem-376	6	7	confirmed	confirm	VERB
eurjchem-376	6	8	and	and	CCONJ
eurjchem-376	6	9	characterized	characterize	VERB
eurjchem-376	6	10	by	by	ADP
eurjchem-376	6	11	the	the	DET
eurjchem-376	6	12	elemental	elemental	ADJ
eurjchem-376	6	13	analysis	analysis	NOUN
eurjchem-376	6	14	and	and	CCONJ
eurjchem-376	6	15	spectroscopic	spectroscopic	NOUN
eurjchem-376	6	16	studies	study	NOUN
eurjchem-376	6	17	(	(	PUNCT
eurjchem-376	6	18	ir	ir	PROPN
eurjchem-376	6	19	,	,	PUNCT
eurjchem-376	6	20	ms	ms	PROPN
eurjchem-376	6	21	,	,	PUNCT
eurjchem-376	6	22	1h	1h	NUM
eurjchem-376	6	23	nmr	nmr	NOUN
eurjchem-376	6	24	,	,	PUNCT
eurjchem-376	6	25	13c	13c	NOUN
eurjchem-376	6	26	nmr	nmr	NOUN
eurjchem-376	6	27	)	)	PUNCT
eurjchem-376	6	28	.	.	PUNCT
eurjchem-376	7	1	dibenzothiophene	dibenzothiophene	VERB
eurjchem-376	7	2	pyridazine	pyridazine	PROPN
eurjchem-376	7	3	triazole	triazole	NOUN
eurjchem-376	7	4	pyrimidinone	pyrimidinone	NOUN
eurjchem-376	7	5	pyrazole	pyrazole	NOUN
eurjchem-376	7	6	pyridinone	pyridinone	NOUN
eurjchem-376	7	7	1	1	NUM
eurjchem-376	7	8	.	.	PUNCT
eurjchem-376	8	1	introduction	introduction	NOUN
eurjchem-376	8	2	nitrogen	nitrogen	NOUN
eurjchem-376	8	3	and	and	CCONJ
eurjchem-376	8	4	sulfur‐containing	sulfur‐containe	VERB
eurjchem-376	8	5	heterocycles	heterocycle	NOUN
eurjchem-376	8	6	have	have	AUX
eurjchem-376	8	7	received	receive	VERB
eurjchem-376	8	8	a	a	DET
eurjchem-376	8	9	great	great	ADJ
eurjchem-376	8	10	deal	deal	NOUN
eurjchem-376	8	11	of	of	ADP
eurjchem-376	8	12	interest	interest	NOUN
eurjchem-376	8	13	in	in	ADP
eurjchem-376	8	14	the	the	DET
eurjchem-376	8	15	biological	biological	ADJ
eurjchem-376	8	16	and	and	CCONJ
eurjchem-376	8	17	medicinal	medicinal	ADJ
eurjchem-376	8	18	sciences	science	NOUN
eurjchem-376	8	19	and	and	CCONJ
eurjchem-376	8	20	this	this	PRON
eurjchem-376	8	21	justifies	justify	VERB
eurjchem-376	8	22	continuing	continue	VERB
eurjchem-376	8	23	efforts	effort	NOUN
eurjchem-376	8	24	in	in	ADP
eurjchem-376	8	25	the	the	DET
eurjchem-376	8	26	development	development	NOUN
eurjchem-376	8	27	of	of	ADP
eurjchem-376	8	28	new	new	ADJ
eurjchem-376	8	29	efficient	efficient	ADJ
eurjchem-376	8	30	and	and	CCONJ
eurjchem-376	8	31	mild	mild	ADJ
eurjchem-376	8	32	synthetic	synthetic	ADJ
eurjchem-376	8	33	strategies	strategy	NOUN
eurjchem-376	8	34	for	for	ADP
eurjchem-376	8	35	their	their	PRON
eurjchem-376	8	36	synthesis	synthesis	NOUN
eurjchem-376	8	37	.	.	PUNCT
eurjchem-376	9	1	among	among	ADP
eurjchem-376	9	2	a	a	DET
eurjchem-376	9	3	large	large	ADJ
eurjchem-376	9	4	variety	variety	NOUN
eurjchem-376	9	5	of	of	ADP
eurjchem-376	9	6	nitrogen	nitrogen	NOUN
eurjchem-376	9	7	containing	contain	VERB
eurjchem-376	9	8	heterocyclic	heterocyclic	ADJ
eurjchem-376	9	9	compounds	compound	NOUN
eurjchem-376	9	10	,	,	PUNCT
eurjchem-376	9	11	pyridazines	pyridazine	NOUN
eurjchem-376	9	12	have	have	AUX
eurjchem-376	9	13	received	receive	VERB
eurjchem-376	9	14	considerable	considerable	ADJ
eurjchem-376	9	15	attention	attention	NOUN
eurjchem-376	9	16	because	because	SCONJ
eurjchem-376	9	17	of	of	ADP
eurjchem-376	9	18	their	their	PRON
eurjchem-376	9	19	pharmacological	pharmacological	ADJ
eurjchem-376	9	20	properties	property	NOUN
eurjchem-376	9	21	and	and	CCONJ
eurjchem-376	9	22	clinical	clinical	ADJ
eurjchem-376	9	23	applications	application	NOUN
eurjchem-376	9	24	[	[	X
eurjchem-376	9	25	1‐9	1‐9	X
eurjchem-376	9	26	]	]	X
eurjchem-376	9	27	.	.	PUNCT
eurjchem-376	10	1	for	for	ADP
eurjchem-376	10	2	example	example	NOUN
eurjchem-376	10	3	,	,	PUNCT
eurjchem-376	10	4	3‐amino‐6‐aryl‐pyridazines	3‐amino‐6‐aryl‐pyridazine	NOUN
eurjchem-376	10	5	were	be	AUX
eurjchem-376	10	6	reported	report	VERB
eurjchem-376	10	7	to	to	PART
eurjchem-376	10	8	possess	possess	VERB
eurjchem-376	10	9	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-376	10	10	and	and	CCONJ
eurjchem-376	10	11	analgesic	analgesic	ADJ
eurjchem-376	10	12	properties	property	NOUN
eurjchem-376	10	13	[	[	X
eurjchem-376	10	14	7	7	NUM
eurjchem-376	10	15	]	]	PUNCT
eurjchem-376	10	16	.	.	PUNCT
eurjchem-376	11	1	also	also	ADV
eurjchem-376	11	2	,	,	PUNCT
eurjchem-376	11	3	pyridazine	pyridazine	NOUN
eurjchem-376	11	4	derivatives	derivative	NOUN
eurjchem-376	11	5	possess	possess	VERB
eurjchem-376	11	6	antiviral	antiviral	NOUN
eurjchem-376	11	7	and	and	CCONJ
eurjchem-376	11	8	anticancer	anticancer	NOUN
eurjchem-376	11	9	[	[	X
eurjchem-376	11	10	10‐12	10‐12	NUM
eurjchem-376	11	11	]	]	PUNCT
eurjchem-376	11	12	,	,	PUNCT
eurjchem-376	11	13	antituberculosis	antituberculosis	NOUN
eurjchem-376	11	14	[	[	X
eurjchem-376	11	15	13	13	NUM
eurjchem-376	11	16	]	]	PUNCT
eurjchem-376	11	17	,	,	PUNCT
eurjchem-376	11	18	antihypertensive	antihypertensive	ADJ
eurjchem-376	11	19	[	[	X
eurjchem-376	11	20	14,15	14,15	NUM
eurjchem-376	11	21	]	]	PUNCT
eurjchem-376	11	22	and	and	CCONJ
eurjchem-376	11	23	antimicrobial	antimicrobial	ADJ
eurjchem-376	11	24	[	[	X
eurjchem-376	11	25	16‐19	16‐19	NUM
eurjchem-376	11	26	]	]	PUNCT
eurjchem-376	11	27	activity	activity	NOUN
eurjchem-376	11	28	.	.	PUNCT
eurjchem-376	12	1	on	on	ADP
eurjchem-376	12	2	the	the	DET
eurjchem-376	12	3	other	other	ADJ
eurjchem-376	12	4	hand	hand	NOUN
eurjchem-376	12	5	,	,	PUNCT
eurjchem-376	12	6	6‐alkoxy‐[1,2,4]triazolo[4,3‐b]pyridazines	6‐alkoxy‐[1,2,4]triazolo[4,3‐b]pyridazines	PROPN
eurjchem-376	12	7	have	have	AUX
eurjchem-376	12	8	been	be	AUX
eurjchem-376	12	9	reported	report	VERB
eurjchem-376	12	10	to	to	PART
eurjchem-376	12	11	possess	possess	VERB
eurjchem-376	12	12	anticonvulsant	anticonvulsant	ADJ
eurjchem-376	12	13	properties	property	NOUN
eurjchem-376	12	14	[	[	X
eurjchem-376	12	15	20	20	NUM
eurjchem-376	12	16	]	]	PUNCT
eurjchem-376	12	17	.	.	PUNCT
eurjchem-376	13	1	based	base	VERB
eurjchem-376	13	2	on	on	ADP
eurjchem-376	13	3	the	the	DET
eurjchem-376	13	4	reported	report	VERB
eurjchem-376	13	5	observations	observation	NOUN
eurjchem-376	13	6	and	and	CCONJ
eurjchem-376	13	7	in	in	ADP
eurjchem-376	13	8	continuation	continuation	NOUN
eurjchem-376	13	9	of	of	ADP
eurjchem-376	13	10	our	our	PRON
eurjchem-376	13	11	research	research	NOUN
eurjchem-376	13	12	interest	interest	NOUN
eurjchem-376	13	13	for	for	ADP
eurjchem-376	13	14	the	the	DET
eurjchem-376	13	15	synthesis	synthesis	NOUN
eurjchem-376	13	16	of	of	ADP
eurjchem-376	13	17	biologically	biologically	ADV
eurjchem-376	13	18	active	active	ADJ
eurjchem-376	13	19	heterocycles	heterocycle	NOUN
eurjchem-376	13	20	[	[	X
eurjchem-376	13	21	21‐24	21‐24	NUM
eurjchem-376	13	22	]	]	X
eurjchem-376	13	23	,	,	PUNCT
eurjchem-376	13	24	the	the	DET
eurjchem-376	13	25	aim	aim	NOUN
eurjchem-376	13	26	of	of	ADP
eurjchem-376	13	27	this	this	DET
eurjchem-376	13	28	study	study	NOUN
eurjchem-376	13	29	is	be	AUX
eurjchem-376	13	30	to	to	PART
eurjchem-376	13	31	design	design	VERB
eurjchem-376	13	32	simple	simple	ADJ
eurjchem-376	13	33	route	route	NOUN
eurjchem-376	13	34	for	for	ADP
eurjchem-376	13	35	the	the	DET
eurjchem-376	13	36	synthesis	synthesis	NOUN
eurjchem-376	13	37	of	of	ADP
eurjchem-376	13	38	pyrazoles	pyrazole	NOUN
eurjchem-376	13	39	,	,	PUNCT
eurjchem-376	13	40	triazoles	triazole	NOUN
eurjchem-376	13	41	,	,	PUNCT
eurjchem-376	13	42	pyridinones	pyridinone	NOUN
eurjchem-376	13	43	and	and	CCONJ
eurjchem-376	13	44	pyrimidinones	pyrimidinone	NOUN
eurjchem-376	13	45	derivatives	derivative	NOUN
eurjchem-376	13	46	attached	attach	VERB
eurjchem-376	13	47	to	to	ADP
eurjchem-376	13	48	pyridazine	pyridazine	NOUN
eurjchem-376	13	49	moiety	moiety	NOUN
eurjchem-376	13	50	.	.	PUNCT
eurjchem-376	14	1	2	2	X
eurjchem-376	14	2	.	.	X
eurjchem-376	14	3	experimental	experimental	ADJ
eurjchem-376	14	4	2.1	2.1	NUM
eurjchem-376	14	5	.	.	PUNCT
eurjchem-376	15	1	synthesis	synthesis	NOUN
eurjchem-376	15	2	2.1.1	2.1.1	NUM
eurjchem-376	15	3	.	.	PUNCT
eurjchem-376	16	1	ethyl	ethyl	PROPN
eurjchem-376	16	2	3‐(6‐dibenzothiophen‐2‐yl‐pyridazin‐3‐ylamino)‐	3‐(6‐dibenzothiophen‐2‐yl‐pyridazin‐3‐ylamino)‐	NUM
eurjchem-376	17	1	3‐oxopropanoate	3‐oxopropanoate	NUM
eurjchem-376	17	2	(	(	PUNCT
eurjchem-376	17	3	2	2	NUM
eurjchem-376	17	4	)	)	PUNCT
eurjchem-376	17	5	a	a	DET
eurjchem-376	17	6	mixture	mixture	NOUN
eurjchem-376	17	7	of	of	ADP
eurjchem-376	17	8	an	an	DET
eurjchem-376	17	9	equimolar	equimolar	NOUN
eurjchem-376	17	10	amount	amount	NOUN
eurjchem-376	17	11	of	of	ADP
eurjchem-376	17	12	aminopyridazine	aminopyridazine	NOUN
eurjchem-376	17	13	1	1	NUM
eurjchem-376	18	1	[	[	X
eurjchem-376	18	2	25	25	NUM
eurjchem-376	18	3	]	]	PUNCT
eurjchem-376	18	4	and	and	CCONJ
eurjchem-376	18	5	diethylmalonate	diethylmalonate	ADJ
eurjchem-376	18	6	(	(	PUNCT
eurjchem-376	18	7	0.01	0.01	NUM
eurjchem-376	18	8	mol	mol	NOUN
eurjchem-376	18	9	)	)	PUNCT
eurjchem-376	18	10	was	be	AUX
eurjchem-376	18	11	heated	heat	VERB
eurjchem-376	18	12	in	in	ADP
eurjchem-376	18	13	an	an	DET
eurjchem-376	18	14	oil	oil	NOUN
eurjchem-376	18	15	bath	bath	NOUN
eurjchem-376	18	16	at	at	ADP
eurjchem-376	18	17	180	180	NUM
eurjchem-376	18	18	oc	oc	NOUN
eurjchem-376	18	19	for	for	ADP
eurjchem-376	18	20	2	2	NUM
eurjchem-376	18	21	hours	hour	NOUN
eurjchem-376	18	22	then	then	ADV
eurjchem-376	18	23	left	leave	VERB
eurjchem-376	18	24	to	to	PART
eurjchem-376	18	25	cool	cool	ADJ
eurjchem-376	18	26	.	.	PUNCT
eurjchem-376	19	1	the	the	DET
eurjchem-376	19	2	product	product	NOUN
eurjchem-376	19	3	was	be	AUX
eurjchem-376	19	4	collected	collect	VERB
eurjchem-376	19	5	and	and	CCONJ
eurjchem-376	19	6	purified	purified	ADJ
eurjchem-376	19	7	:	:	PUNCT
eurjchem-376	19	8	yellow	yellow	ADJ
eurjchem-376	19	9	,	,	PUNCT
eurjchem-376	19	10	yield	yield	NOUN
eurjchem-376	19	11	:	:	PUNCT
eurjchem-376	19	12	80	80	NUM
eurjchem-376	19	13	%	%	NOUN
eurjchem-376	19	14	,	,	PUNCT
eurjchem-376	19	15	(	(	PUNCT
eurjchem-376	19	16	ethanol	ethanol	NOUN
eurjchem-376	19	17	)	)	PUNCT
eurjchem-376	19	18	(	(	PUNCT
eurjchem-376	19	19	scheme	scheme	NOUN
eurjchem-376	19	20	1	1	NUM
eurjchem-376	19	21	)	)	PUNCT
eurjchem-376	19	22	.	.	PUNCT
eurjchem-376	20	1	m.p	m.p	PROPN
eurjchem-376	20	2	.	.	PROPN
eurjchem-376	20	3	:	:	PUNCT
eurjchem-376	21	1	176‐178	176‐178	NUM
eurjchem-376	21	2	c	c	ADJ
eurjchem-376	21	3	.	.	PUNCT
eurjchem-376	22	1	ir	ir	PROPN
eurjchem-376	22	2	(	(	PUNCT
eurjchem-376	22	3	kbr	kbr	PROPN
eurjchem-376	22	4	,	,	PUNCT
eurjchem-376	22	5	cm‐1	cm‐1	PROPN
eurjchem-376	22	6	):	):	PUNCT
eurjchem-376	22	7	3390‐3280	3390‐3280	NUM
eurjchem-376	22	8	(nh	(nh	NOUN
eurjchem-376	22	9	)	)	PUNCT
eurjchem-376	22	10	,	,	PUNCT
eurjchem-376	22	11	2950	2950	NUM
eurjchem-376	22	12	,	,	PUNCT
eurjchem-376	22	13	2880	2880	NUM
eurjchem-376	22	14	(ch2	(ch2	NOUN
eurjchem-376	22	15	)	)	PUNCT
eurjchem-376	22	16	,	,	PUNCT
eurjchem-376	22	17	1730	1730	NUM
eurjchem-376	22	18	,	,	PUNCT
eurjchem-376	22	19	1685	1685	NUM
eurjchem-376	22	20	(co	(co	NOUN
eurjchem-376	22	21	)	)	PUNCT
eurjchem-376	22	22	,	,	PUNCT
eurjchem-376	22	23	1630	1630	NUM
eurjchem-376	22	24	(c	(c	PROPN
eurjchem-376	22	25	=	=	SYM
eurjchem-376	22	26	n	n	NUM
eurjchem-376	22	27	)	)	PUNCT
eurjchem-376	22	28	.	.	PUNCT
eurjchem-376	23	1	1h	1h	NUM
eurjchem-376	23	2	nmr	nmr	NOUN
eurjchem-376	23	3	(	(	PUNCT
eurjchem-376	23	4	200	200	NUM
eurjchem-376	23	5	mhz	mhz	NOUN
eurjchem-376	23	6	,	,	PUNCT
eurjchem-376	23	7	cdcl3	cdcl3	NOUN
eurjchem-376	23	8	):	):	PUNCT
eurjchem-376	23	9	1.32	1.32	NUM
eurjchem-376	23	10	(	(	PUNCT
eurjchem-376	23	11	t	t	PROPN
eurjchem-376	23	12	,	,	PUNCT
eurjchem-376	23	13	3h	3h	NUM
eurjchem-376	23	14	,	,	PUNCT
eurjchem-376	23	15	ch3	ch3	PROPN
eurjchem-376	23	16	)	)	PUNCT
eurjchem-376	23	17	,	,	PUNCT
eurjchem-376	23	18	4.31	4.31	NUM
eurjchem-376	23	19	(	(	PUNCT
eurjchem-376	23	20	q	q	NOUN
eurjchem-376	23	21	,	,	PUNCT
eurjchem-376	23	22	2h	2h	NUM
eurjchem-376	23	23	,	,	PUNCT
eurjchem-376	23	24	ch2	ch2	PROPN
eurjchem-376	23	25	)	)	PUNCT
eurjchem-376	23	26	,	,	PUNCT
eurjchem-376	23	27	5.40	5.40	NUM
eurjchem-376	23	28	(	(	PUNCT
eurjchem-376	23	29	s	s	PROPN
eurjchem-376	23	30	,	,	PUNCT
eurjchem-376	23	31	2h	2h	NUM
eurjchem-376	23	32	,	,	PUNCT
eurjchem-376	23	33	ch2	ch2	PROPN
eurjchem-376	23	34	)	)	PUNCT
eurjchem-376	23	35	,	,	PUNCT
eurjchem-376	23	36	8.62	8.62	NUM
eurjchem-376	23	37	(	(	PUNCT
eurjchem-376	23	38	s	s	PROPN
eurjchem-376	23	39	,	,	PUNCT
eurjchem-376	23	40	1h	1h	NUM
eurjchem-376	23	41	,	,	PUNCT
eurjchem-376	23	42	nh	nh	PROPN
eurjchem-376	23	43	,	,	PUNCT
eurjchem-376	23	44	exchangeable	exchangeable	ADJ
eurjchem-376	23	45	)	)	PUNCT
eurjchem-376	23	46	,	,	PUNCT
eurjchem-376	23	47	6.91‐7.96	6.91‐7.96	NUM
eurjchem-376	23	48	(	(	PUNCT
eurjchem-376	23	49	m	m	PROPN
eurjchem-376	23	50	,	,	PUNCT
eurjchem-376	23	51	9h	9h	NUM
eurjchem-376	23	52	,	,	PUNCT
eurjchem-376	23	53	ar‐h	ar‐h	NOUN
eurjchem-376	23	54	)	)	PUNCT
eurjchem-376	23	55	.	.	PUNCT
eurjchem-376	24	1	13c	13c	NOUN
eurjchem-376	24	2	nmr	nmr	NOUN
eurjchem-376	24	3	(	(	PUNCT
eurjchem-376	24	4	50	50	NUM
eurjchem-376	24	5	mhz	mhz	NOUN
eurjchem-376	24	6	,	,	PUNCT
eurjchem-376	24	7	cdcl3	cdcl3	NOUN
eurjchem-376	24	8	):	):	PUNCT
eurjchem-376	24	9	17.2	17.2	NUM
eurjchem-376	24	10	(	(	PUNCT
eurjchem-376	24	11	ch3	ch3	PROPN
eurjchem-376	24	12	)	)	PUNCT
eurjchem-376	24	13	,	,	PUNCT
eurjchem-376	24	14	54.3	54.3	NUM
eurjchem-376	24	15	(	(	PUNCT
eurjchem-376	24	16	ch2	ch2	NOUN
eurjchem-376	24	17	ester	ester	NOUN
eurjchem-376	24	18	)	)	PUNCT
eurjchem-376	24	19	,	,	PUNCT
eurjchem-376	24	20	47.1	47.1	NUM
eurjchem-376	24	21	(	(	PUNCT
eurjchem-376	24	22	ch2	ch2	PROPN
eurjchem-376	24	23	)	)	PUNCT
eurjchem-376	24	24	,	,	PUNCT
eurjchem-376	24	25	119.2	119.2	NUM
eurjchem-376	24	26	,	,	PUNCT
eurjchem-376	24	27	121.3	121.3	NUM
eurjchem-376	24	28	,	,	PUNCT
eurjchem-376	24	29	121.8	121.8	NUM
eurjchem-376	24	30	,	,	PUNCT
eurjchem-376	24	31	122.6	122.6	NUM
eurjchem-376	24	32	,	,	PUNCT
eurjchem-376	24	33	123.1	123.1	NUM
eurjchem-376	24	34	,	,	PUNCT
eurjchem-376	24	35	123.7	123.7	NUM
eurjchem-376	24	36	,	,	PUNCT
eurjchem-376	24	37	124.2	124.2	NUM
eurjchem-376	24	38	,	,	PUNCT
eurjchem-376	24	39	124.6	124.6	NUM
eurjchem-376	24	40	,	,	PUNCT
eurjchem-376	24	41	126.3	126.3	NUM
eurjchem-376	24	42	,	,	PUNCT
eurjchem-376	24	43	127.6	127.6	NUM
eurjchem-376	24	44	,	,	PUNCT
eurjchem-376	24	45	128.1	128.1	NUM
eurjchem-376	24	46	,	,	PUNCT
eurjchem-376	24	47	132.5	132.5	NUM
eurjchem-376	24	48	,	,	PUNCT
eurjchem-376	24	49	138.3	138.3	NUM
eurjchem-376	24	50	,	,	PUNCT
eurjchem-376	24	51	139.1	139.1	NUM
eurjchem-376	24	52	,	,	PUNCT
eurjchem-376	24	53	148.7	148.7	NUM
eurjchem-376	24	54	,	,	PUNCT
eurjchem-376	24	55	151.1	151.1	NUM
eurjchem-376	24	56	(	(	PUNCT
eurjchem-376	24	57	dibenzothiophene	dibenzothiophene	ADJ
eurjchem-376	24	58	and	and	CCONJ
eurjchem-376	24	59	pyridazine	pyridazine	NOUN
eurjchem-376	24	60	carbons	carbon	NOUN
eurjchem-376	24	61	)	)	PUNCT
eurjchem-376	24	62	,	,	PUNCT
eurjchem-376	24	63	172.2	172.2	NUM
eurjchem-376	24	64	,	,	PUNCT
eurjchem-376	24	65	175.4	175.4	NUM
eurjchem-376	24	66	(	(	PUNCT
eurjchem-376	24	67	2co	2co	NOUN
eurjchem-376	24	68	)	)	PUNCT
eurjchem-376	24	69	.	.	PUNCT
eurjchem-376	25	1	ms	ms	NOUN
eurjchem-376	25	2	(	(	PUNCT
eurjchem-376	25	3	m	m	PROPN
eurjchem-376	25	4	/	/	SYM
eurjchem-376	25	5	z	z	NOUN
eurjchem-376	25	6	):	):	PUNCT
eurjchem-376	25	7	391	391	NUM
eurjchem-376	25	8	(	(	PUNCT
eurjchem-376	25	9	m+	m+	NUM
eurjchem-376	25	10	)	)	PUNCT
eurjchem-376	25	11	.	.	PUNCT
eurjchem-376	26	1	anal	anal	PROPN
eurjchem-376	26	2	.	.	PUNCT
eurjchem-376	26	3	calcd	calcd	NOUN
eurjchem-376	26	4	.	.	PUNCT
eurjchem-376	27	1	for	for	SCONJ
eurjchem-376	27	2	c21h17n3o3s	c21h17n3o3s	NUM
eurjchem-376	27	3	:	:	PUNCT
eurjchem-376	27	4	c	c	X
eurjchem-376	27	5	,	,	PUNCT
eurjchem-376	27	6	64.43	64.43	NUM
eurjchem-376	27	7	;	;	PUNCT
eurjchem-376	27	8	h	h	NOUN
eurjchem-376	27	9	,	,	PUNCT
eurjchem-376	27	10	4.38	4.38	NUM
eurjchem-376	27	11	;	;	PUNCT
eurjchem-376	27	12	n	n	CCONJ
eurjchem-376	27	13	,	,	PUNCT
eurjchem-376	27	14	10.73	10.73	NUM
eurjchem-376	27	15	.	.	PUNCT
eurjchem-376	27	16	found	find	VERB
eurjchem-376	27	17	:	:	PUNCT
eurjchem-376	28	1	c	c	X
eurjchem-376	28	2	,	,	PUNCT
eurjchem-376	28	3	64.28	64.28	NUM
eurjchem-376	28	4	;	;	PUNCT
eurjchem-376	28	5	h	h	NOUN
eurjchem-376	28	6	,	,	PUNCT
eurjchem-376	28	7	4.25	4.25	NUM
eurjchem-376	28	8	;	;	PUNCT
eurjchem-376	28	9	n	n	CCONJ
eurjchem-376	28	10	,	,	PUNCT
eurjchem-376	28	11	10.56	10.56	NUM
eurjchem-376	28	12	%	%	NOUN
eurjchem-376	28	13	.	.	PUNCT
eurjchem-376	29	1	scheme	scheme	VERB
eurjchem-376	29	2	1	1	NUM
eurjchem-376	29	3	2.1.2	2.1.2	NUM
eurjchem-376	29	4	.	.	PUNCT
eurjchem-376	29	5	ethyl	ethyl	PROPN
eurjchem-376	29	6	2‐(6‐dibenzothiophen‐2‐yl	2‐(6‐dibenzothiophen‐2‐yl	PROPN
eurjchem-376	29	7	–	–	PUNCT
eurjchem-376	29	8	pyridazin‐3‐yl	pyridazin‐3‐yl	NOUN
eurjchem-376	29	9	carbamoyl)‐3‐phenylacrylate	carbamoyl)‐3‐phenylacrylate	X
eurjchem-376	29	10	(	(	PUNCT
eurjchem-376	29	11	3	3	NUM
eurjchem-376	29	12	)	)	PUNCT
eurjchem-376	29	13	benzaldehyde	benzaldehyde	NOUN
eurjchem-376	29	14	(	(	PUNCT
eurjchem-376	29	15	0.01	0.01	NUM
eurjchem-376	29	16	mol	mol	NOUN
eurjchem-376	29	17	)	)	PUNCT
eurjchem-376	29	18	was	be	AUX
eurjchem-376	29	19	added	add	VERB
eurjchem-376	29	20	to	to	ADP
eurjchem-376	29	21	a	a	DET
eurjchem-376	29	22	solution	solution	NOUN
eurjchem-376	29	23	of	of	ADP
eurjchem-376	29	24	ester	ester	NOUN
eurjchem-376	29	25	2	2	NUM
eurjchem-376	29	26	(	(	PUNCT
eurjchem-376	29	27	0.01	0.01	NUM
eurjchem-376	29	28	mol	mol	NOUN
eurjchem-376	29	29	)	)	PUNCT
eurjchem-376	29	30	in	in	ADP
eurjchem-376	29	31	dioxan	dioxan	PROPN
eurjchem-376	29	32	(	(	PUNCT
eurjchem-376	29	33	30	30	NUM
eurjchem-376	29	34	ml	ml	NOUN
eurjchem-376	29	35	)	)	PUNCT
eurjchem-376	29	36	containing	contain	VERB
eurjchem-376	29	37	few	few	ADJ
eurjchem-376	29	38	drops	drop	NOUN
eurjchem-376	29	39	of	of	ADP
eurjchem-376	29	40	piperidine	piperidine	NOUN
eurjchem-376	29	41	.	.	PUNCT
eurjchem-376	30	1	the	the	DET
eurjchem-376	30	2	reaction	reaction	NOUN
eurjchem-376	30	3	mixture	mixture	NOUN
eurjchem-376	30	4	was	be	AUX
eurjchem-376	30	5	heated	heat	VERB
eurjchem-376	30	6	under	under	ADP
eurjchem-376	30	7	reflux	reflux	NOUN
eurjchem-376	30	8	for	for	ADP
eurjchem-376	30	9	3	3	NUM
eurjchem-376	30	10	hours	hour	NOUN
eurjchem-376	30	11	then	then	ADV
eurjchem-376	30	12	the	the	DET
eurjchem-376	30	13	solvent	solvent	NOUN
eurjchem-376	30	14	was	be	AUX
eurjchem-376	30	15	removed	remove	VERB
eurjchem-376	30	16	.	.	PUNCT
eurjchem-376	31	1	the	the	DET
eurjchem-376	31	2	remaining	remain	VERB
eurjchem-376	31	3	residue	residue	NOUN
eurjchem-376	31	4	was	be	AUX
eurjchem-376	31	5	triturated	triturate	VERB
eurjchem-376	31	6	with	with	ADP
eurjchem-376	31	7	petroleum	petroleum	NOUN
eurjchem-376	31	8	ether	ether	NOUN
eurjchem-376	31	9	to	to	PART
eurjchem-376	31	10	give	give	VERB
eurjchem-376	31	11	the	the	DET
eurjchem-376	31	12	solid	solid	ADJ
eurjchem-376	31	13	product	product	NOUN
eurjchem-376	31	14	:	:	PUNCT
eurjchem-376	31	15	yellow	yellow	ADJ
eurjchem-376	31	16	,	,	PUNCT
eurjchem-376	31	17	yield	yield	NOUN
eurjchem-376	31	18	:	:	PUNCT
eurjchem-376	31	19	68	68	NUM
eurjchem-376	31	20	%	%	NOUN
eurjchem-376	31	21	(	(	PUNCT
eurjchem-376	31	22	butanol	butanol	NOUN
eurjchem-376	31	23	)	)	PUNCT
eurjchem-376	31	24	(	(	PUNCT
eurjchem-376	31	25	scheme	scheme	NOUN
eurjchem-376	31	26	2	2	NUM
eurjchem-376	31	27	)	)	PUNCT
eurjchem-376	31	28	.	.	PUNCT
eurjchem-376	32	1	m.p	m.p	PROPN
eurjchem-376	32	2	.	.	PROPN
eurjchem-376	32	3	:	:	PUNCT
eurjchem-376	33	1	197‐199	197‐199	NUM
eurjchem-376	33	2	c	c	ADJ
eurjchem-376	33	3	.	.	PUNCT
eurjchem-376	34	1	ir	ir	PROPN
eurjchem-376	34	2	(	(	PUNCT
eurjchem-376	34	3	kbr	kbr	PROPN
eurjchem-376	34	4	,	,	PUNCT
eurjchem-376	34	5	cm‐1	cm‐1	PROPN
eurjchem-376	34	6	):	):	PUNCT
eurjchem-376	34	7	3360‐3230	3360‐3230	NUM
eurjchem-376	34	8	(nh	(nh	NOUN
eurjchem-376	34	9	)	)	PUNCT
eurjchem-376	34	10	,	,	PUNCT
eurjchem-376	34	11	2940	2940	NUM
eurjchem-376	34	12	,	,	PUNCT
eurjchem-376	34	13	2860	2860	NUM
eurjchem-376	34	14	(ch‐aliphatic	(ch‐aliphatic	PROPN
eurjchem-376	34	15	)	)	PUNCT
eurjchem-376	34	16	1715	1715	NUM
eurjchem-376	34	17	,	,	PUNCT
eurjchem-376	34	18	1670	1670	NUM
eurjchem-376	34	19	(co	(co	NOUN
eurjchem-376	34	20	)	)	PUNCT
eurjchem-376	34	21	,	,	PUNCT
eurjchem-376	34	22	1620	1620	NUM
eurjchem-376	34	23	(c	(c	PROPN
eurjchem-376	34	24	=	=	SYM
eurjchem-376	34	25	c	c	NOUN
eurjchem-376	34	26	)	)	PUNCT
eurjchem-376	34	27	.	.	PUNCT
eurjchem-376	35	1	1h	1h	NUM
eurjchem-376	35	2	nmr	nmr	NOUN
eurjchem-376	35	3	(	(	PUNCT
eurjchem-376	35	4	200	200	NUM
eurjchem-376	35	5	mhz	mhz	NOUN
eurjchem-376	35	6	,	,	PUNCT
eurjchem-376	35	7	cdcl3	cdcl3	NOUN
eurjchem-376	35	8	):	):	PUNCT
eurjchem-376	35	9	1.32	1.32	NUM
eurjchem-376	35	10	(	(	PUNCT
eurjchem-376	35	11	t	t	PROPN
eurjchem-376	35	12	,	,	PUNCT
eurjchem-376	35	13	3h	3h	NUM
eurjchem-376	35	14	,	,	PUNCT
eurjchem-376	35	15	ch3	ch3	PROPN
eurjchem-376	35	16	)	)	PUNCT
eurjchem-376	35	17	,	,	PUNCT
eurjchem-376	35	18	4.20	4.20	NUM
eurjchem-376	35	19	(	(	PUNCT
eurjchem-376	35	20	q	q	NOUN
eurjchem-376	35	21	,	,	PUNCT
eurjchem-376	35	22	2h	2h	NUM
eurjchem-376	35	23	,	,	PUNCT
eurjchem-376	35	24	ch2	ch2	PROPN
eurjchem-376	35	25	)	)	PUNCT
eurjchem-376	35	26	,	,	PUNCT
eurjchem-376	35	27	6.62	6.62	NUM
eurjchem-376	35	28	(	(	PUNCT
eurjchem-376	35	29	s	s	PROPN
eurjchem-376	35	30	,	,	PUNCT
eurjchem-376	35	31	1h	1h	NUM
eurjchem-376	35	32	,	,	PUNCT
eurjchem-376	35	33	c	c	NOUN
eurjchem-376	35	34	=	=	NOUN
eurjchem-376	35	35	ch	ch	NOUN
eurjchem-376	35	36	)	)	PUNCT
eurjchem-376	35	37	,	,	PUNCT
eurjchem-376	35	38	8.81	8.81	NUM
eurjchem-376	35	39	(	(	PUNCT
eurjchem-376	35	40	s	s	PROPN
eurjchem-376	35	41	,	,	PUNCT
eurjchem-376	35	42	296	296	NUM
eurjchem-376	35	43	behalo	behalo	NOUN
eurjchem-376	35	44	and	and	CCONJ
eurjchem-376	35	45	aly	aly	PROPN
eurjchem-376	35	46	/	/	SYM
eurjchem-376	35	47	european	european	PROPN
eurjchem-376	35	48	journal	journal	PROPN
eurjchem-376	35	49	of	of	ADP
eurjchem-376	35	50	chemistry	chemistry	NOUN
eurjchem-376	35	51	2	2	NUM
eurjchem-376	35	52	(	(	PUNCT
eurjchem-376	35	53	3	3	NUM
eurjchem-376	35	54	)	)	PUNCT
eurjchem-376	35	55	(	(	PUNCT
eurjchem-376	35	56	2011	2011	NUM
eurjchem-376	35	57	)	)	PUNCT
eurjchem-376	35	58	295‐299	295‐299	NOUN
eurjchem-376	36	1	nh	nh	NOUN
eurjchem-376	37	1	o	o	X
eurjchem-376	37	2	o	o	X
eurjchem-376	38	1	oc2h5	oc2h5	NOUN
eurjchem-376	38	2	chph	chph	PROPN
eurjchem-376	38	3	nhc	nhc	PROPN
eurjchem-376	38	4	o	o	PROPN
eurjchem-376	38	5	n	n	CCONJ
eurjchem-376	38	6	nr	nr	PROPN
eurjchem-376	38	7	ph	ph	PROPN
eurjchem-376	38	8	oh	oh	INTJ
eurjchem-376	38	9	ar	ar	PROPN
eurjchem-376	38	10	ar	ar	PROPN
eurjchem-376	38	11	3	3	NUM
eurjchem-376	38	12	4a	4a	NUM
eurjchem-376	38	13	,	,	PUNCT
eurjchem-376	38	14	b	b	NOUN
eurjchem-376	38	15	4a	4a	NUM
eurjchem-376	38	16	r	r	NOUN
eurjchem-376	38	17	=	=	SYM
eurjchem-376	38	18	h	h	NOUN
eurjchem-376	38	19	,	,	PUNCT
eurjchem-376	38	20	4b	4b	PROPN
eurjchem-376	38	21	r	r	NOUN
eurjchem-376	38	22	=	=	PUNCT
eurjchem-376	38	23	c6h5	c6h5	PROPN
eurjchem-376	38	24	rnhnh2	rnhnh2	NOUN
eurjchem-376	39	1	2	2	NUM
eurjchem-376	39	2	phcho	phcho	NOUN
eurjchem-376	39	3	nhc	nhc	PROPN
eurjchem-376	39	4	o	o	PROPN
eurjchem-376	40	1	oo	oo	INTJ
eurjchem-376	40	2	cho	cho	NOUN
eurjchem-376	41	1	oh	oh	INTJ
eurjchem-376	41	2	ar	ar	PROPN
eurjchem-376	41	3	5	5	NUM
eurjchem-376	41	4	nh	nh	NOUN
eurjchem-376	41	5	o	o	NOUN
eurjchem-376	41	6	o	o	X
eurjchem-376	42	1	oc2h5	oc2h5	PROPN
eurjchem-376	42	2	n	n	CCONJ
eurjchem-376	42	3	nh	nh	PROPN
eurjchem-376	42	4	ph	ph	PROPN
eurjchem-376	42	5	ar	ar	PROPN
eurjchem-376	42	6	6	6	NUM
eurjchem-376	42	7	nh2nh2	nh2nh2	NOUN
eurjchem-376	42	8	n	n	ADP
eurjchem-376	42	9	n	n	PRON
eurjchem-376	42	10	nphnhc	nphnhc	NOUN
eurjchem-376	42	11	ho	ho	PROPN
eurjchem-376	42	12	o	o	PROPN
eurjchem-376	42	13	ar	ar	PROPN
eurjchem-376	42	14	7	7	NUM
eurjchem-376	42	15	phn2cl	phn2cl	PROPN
eurjchem-376	42	16	scheme	scheme	NOUN
eurjchem-376	42	17	2	2	NUM
eurjchem-376	42	18	1h	1h	NUM
eurjchem-376	42	19	,	,	PUNCT
eurjchem-376	42	20	nh	nh	PROPN
eurjchem-376	42	21	,	,	PUNCT
eurjchem-376	42	22	exchangeable	exchangeable	ADJ
eurjchem-376	42	23	)	)	PUNCT
eurjchem-376	42	24	,	,	PUNCT
eurjchem-376	42	25	6.84‐8.02	6.84‐8.02	NUM
eurjchem-376	42	26	(	(	PUNCT
eurjchem-376	42	27	m	m	PROPN
eurjchem-376	42	28	,	,	PUNCT
eurjchem-376	42	29	14h	14h	NUM
eurjchem-376	42	30	,	,	PUNCT
eurjchem-376	42	31	arh	arh	PROPN
eurjchem-376	42	32	)	)	PUNCT
eurjchem-376	42	33	.	.	PUNCT
eurjchem-376	43	1	13c	13c	NOUN
eurjchem-376	43	2	nmr	nmr	NOUN
eurjchem-376	43	3	(	(	PUNCT
eurjchem-376	43	4	50	50	NUM
eurjchem-376	43	5	mhz	mhz	NOUN
eurjchem-376	43	6	,	,	PUNCT
eurjchem-376	43	7	cdcl3	cdcl3	NOUN
eurjchem-376	43	8	):	):	PUNCT
eurjchem-376	43	9	16.4	16.4	NUM
eurjchem-376	43	10	(	(	PUNCT
eurjchem-376	43	11	ch3	ch3	PROPN
eurjchem-376	43	12	)	)	PUNCT
eurjchem-376	43	13	,	,	PUNCT
eurjchem-376	43	14	55.6	55.6	NUM
eurjchem-376	43	15	(	(	PUNCT
eurjchem-376	43	16	ch2	ch2	NOUN
eurjchem-376	43	17	ester	ester	NOUN
eurjchem-376	43	18	)	)	PUNCT
eurjchem-376	43	19	,	,	PUNCT
eurjchem-376	43	20	123.6	123.6	NUM
eurjchem-376	43	21	(	(	PUNCT
eurjchem-376	43	22	c	c	NOUN
eurjchem-376	43	23	=	=	SYM
eurjchem-376	43	24	chph	chph	ADJ
eurjchem-376	43	25	)	)	PUNCT
eurjchem-376	43	26	,	,	PUNCT
eurjchem-376	43	27	146.2	146.2	NUM
eurjchem-376	43	28	(	(	PUNCT
eurjchem-376	43	29	c	c	NOUN
eurjchem-376	43	30	=	=	SYM
eurjchem-376	43	31	chph	chph	ADJ
eurjchem-376	43	32	)	)	PUNCT
eurjchem-376	43	33	,	,	PUNCT
eurjchem-376	43	34	125.6	125.6	NUM
eurjchem-376	43	35	,	,	PUNCT
eurjchem-376	43	36	127.3	127.3	NUM
eurjchem-376	43	37	,	,	PUNCT
eurjchem-376	43	38	128.2	128.2	NUM
eurjchem-376	43	39	,	,	PUNCT
eurjchem-376	43	40	135.5	135.5	NUM
eurjchem-376	43	41	(	(	PUNCT
eurjchem-376	43	42	phenyl	phenyl	NOUN
eurjchem-376	43	43	carbons	carbon	NOUN
eurjchem-376	43	44	,	,	PUNCT
eurjchem-376	43	45	in	in	ADP
eurjchem-376	43	46	addition	addition	NOUN
eurjchem-376	43	47	to	to	PART
eurjchem-376	43	48	dibenzothiophene	dibenzothiophene	VERB
eurjchem-376	43	49	and	and	CCONJ
eurjchem-376	43	50	pyridazine	pyridazine	NOUN
eurjchem-376	43	51	carbons	carbon	NOUN
eurjchem-376	43	52	)	)	PUNCT
eurjchem-376	43	53	.	.	PUNCT
eurjchem-376	44	1	ms	ms	NOUN
eurjchem-376	44	2	(	(	PUNCT
eurjchem-376	44	3	m	m	PROPN
eurjchem-376	44	4	/	/	SYM
eurjchem-376	44	5	z	z	ADJ
eurjchem-376	44	6	):	):	PUNCT
eurjchem-376	44	7	479	479	NUM
eurjchem-376	44	8	(	(	PUNCT
eurjchem-376	44	9	m+	m+	NUM
eurjchem-376	44	10	)	)	PUNCT
eurjchem-376	44	11	.	.	PUNCT
eurjchem-376	45	1	anal	anal	PROPN
eurjchem-376	45	2	.	.	PUNCT
eurjchem-376	45	3	calcd	calcd	NOUN
eurjchem-376	45	4	.	.	PUNCT
eurjchem-376	46	1	for	for	SCONJ
eurjchem-376	46	2	c28h21n3o3s	c28h21n3o3s	NUM
eurjchem-376	46	3	:	:	PUNCT
eurjchem-376	46	4	c	c	X
eurjchem-376	46	5	,	,	PUNCT
eurjchem-376	46	6	70.13	70.13	NUM
eurjchem-376	46	7	;	;	PUNCT
eurjchem-376	46	8	h	h	NOUN
eurjchem-376	46	9	,	,	PUNCT
eurjchem-376	46	10	4.41	4.41	NUM
eurjchem-376	46	11	;	;	PUNCT
eurjchem-376	46	12	n	n	CCONJ
eurjchem-376	46	13	,	,	PUNCT
eurjchem-376	46	14	8.76	8.76	NUM
eurjchem-376	46	15	.	.	PUNCT
eurjchem-376	46	16	found	find	VERB
eurjchem-376	46	17	:	:	PUNCT
eurjchem-376	47	1	c	c	X
eurjchem-376	47	2	,	,	PUNCT
eurjchem-376	47	3	70.27	70.27	NUM
eurjchem-376	47	4	;	;	PUNCT
eurjchem-376	47	5	h	h	NOUN
eurjchem-376	47	6	,	,	PUNCT
eurjchem-376	47	7	4.52	4.52	NUM
eurjchem-376	47	8	;	;	PUNCT
eurjchem-376	47	9	n	n	CCONJ
eurjchem-376	47	10	,	,	PUNCT
eurjchem-376	47	11	8.58	8.58	NUM
eurjchem-376	47	12	%	%	NOUN
eurjchem-376	47	13	.	.	PUNCT
eurjchem-376	48	1	2.1.3	2.1.3	X
eurjchem-376	48	2	.	.	PUNCT
eurjchem-376	48	3	general	general	ADJ
eurjchem-376	48	4	procedure	procedure	NOUN
eurjchem-376	48	5	for	for	ADP
eurjchem-376	48	6	the	the	DET
eurjchem-376	48	7	synthesis	synthesis	NOUN
eurjchem-376	48	8	of	of	ADP
eurjchem-376	48	9	4a	4a	NUM
eurjchem-376	48	10	,	,	PUNCT
eurjchem-376	48	11	b	b	NOUN
eurjchem-376	48	12	a	a	DET
eurjchem-376	48	13	mixture	mixture	NOUN
eurjchem-376	48	14	of	of	ADP
eurjchem-376	48	15	3	3	NUM
eurjchem-376	48	16	(	(	PUNCT
eurjchem-376	48	17	0.01	0.01	NUM
eurjchem-376	48	18	mol	mol	NOUN
eurjchem-376	48	19	)	)	PUNCT
eurjchem-376	48	20	and	and	CCONJ
eurjchem-376	48	21	hydrazine	hydrazine	NOUN
eurjchem-376	48	22	hydrate	hydrate	NOUN
eurjchem-376	48	23	or	or	CCONJ
eurjchem-376	48	24	phenyl‐	phenyl‐	NOUN
eurjchem-376	48	25	hydrazine	hydrazine	NOUN
eurjchem-376	48	26	(	(	PUNCT
eurjchem-376	48	27	0.01	0.01	NUM
eurjchem-376	48	28	mol	mol	NOUN
eurjchem-376	48	29	)	)	PUNCT
eurjchem-376	48	30	was	be	AUX
eurjchem-376	48	31	heated	heat	VERB
eurjchem-376	48	32	in	in	ADP
eurjchem-376	48	33	ethanol	ethanol	NOUN
eurjchem-376	48	34	(	(	PUNCT
eurjchem-376	48	35	30	30	NUM
eurjchem-376	48	36	ml	ml	NOUN
eurjchem-376	48	37	)	)	PUNCT
eurjchem-376	48	38	under	under	ADP
eurjchem-376	48	39	reflux	reflux	NOUN
eurjchem-376	48	40	for	for	ADP
eurjchem-376	48	41	3	3	NUM
eurjchem-376	48	42	hours	hour	NOUN
eurjchem-376	48	43	then	then	ADV
eurjchem-376	48	44	left	leave	VERB
eurjchem-376	48	45	to	to	PART
eurjchem-376	48	46	cool	cool	ADJ
eurjchem-376	48	47	.	.	PUNCT
eurjchem-376	49	1	the	the	DET
eurjchem-376	49	2	formed	form	VERB
eurjchem-376	49	3	solid	solid	ADJ
eurjchem-376	49	4	product	product	NOUN
eurjchem-376	49	5	was	be	AUX
eurjchem-376	49	6	collected	collect	VERB
eurjchem-376	49	7	by	by	ADP
eurjchem-376	49	8	filtration	filtration	NOUN
eurjchem-376	49	9	and	and	CCONJ
eurjchem-376	49	10	recrystallized	recrystallize	VERB
eurjchem-376	49	11	(	(	PUNCT
eurjchem-376	49	12	scheme	scheme	NOUN
eurjchem-376	49	13	2	2	NUM
eurjchem-376	49	14	)	)	PUNCT
eurjchem-376	49	15	.	.	PUNCT
eurjchem-376	50	1	n‐(6‐dibenzothiophen‐2‐yl	n‐(6‐dibenzothiophen‐2‐yl	PROPN
eurjchem-376	50	2	–	–	PUNCT
eurjchem-376	50	3	pyridazin‐3‐yl)‐3‐hydroxy‐5‐	pyridazin‐3‐yl)‐3‐hydroxy‐5‐	NOUN
eurjchem-376	50	4	phenyl‐1h‐pyrazole‐4‐carboxamide	phenyl‐1h‐pyrazole‐4‐carboxamide	NOUN
eurjchem-376	50	5	(	(	PUNCT
eurjchem-376	50	6	4a	4a	NOUN
eurjchem-376	50	7	):	):	PUNCT
eurjchem-376	50	8	yellow	yellow	ADJ
eurjchem-376	50	9	,	,	PUNCT
eurjchem-376	50	10	yield	yield	NOUN
eurjchem-376	50	11	:	:	PUNCT
eurjchem-376	50	12	81	81	NUM
eurjchem-376	50	13	%	%	NOUN
eurjchem-376	50	14	(	(	PUNCT
eurjchem-376	50	15	ethanol	ethanol	NOUN
eurjchem-376	50	16	)	)	PUNCT
eurjchem-376	50	17	.	.	PUNCT
eurjchem-376	51	1	m.p	m.p	PROPN
eurjchem-376	51	2	.	.	PROPN
eurjchem-376	51	3	:	:	PUNCT
eurjchem-376	52	1	180‐182	180‐182	PROPN
eurjchem-376	52	2	c	c	ADJ
eurjchem-376	52	3	.	.	PUNCT
eurjchem-376	53	1	ir	ir	PROPN
eurjchem-376	53	2	(	(	PUNCT
eurjchem-376	53	3	kbr	kbr	PROPN
eurjchem-376	53	4	,	,	PUNCT
eurjchem-376	53	5	cm‐1	cm‐1	PROPN
eurjchem-376	53	6	):	):	PUNCT
eurjchem-376	53	7	3490‐3240	3490‐3240	NUM
eurjchem-376	53	8	(oh	(oh	NOUN
eurjchem-376	53	9	,	,	PUNCT
eurjchem-376	53	10	nh	nh	PROPN
eurjchem-376	53	11	)	)	PUNCT
eurjchem-376	53	12	,	,	PUNCT
eurjchem-376	53	13	1685	1685	NUM
eurjchem-376	53	14	(co	(co	NOUN
eurjchem-376	53	15	)	)	PUNCT
eurjchem-376	53	16	,	,	PUNCT
eurjchem-376	53	17	1650	1650	NUM
eurjchem-376	53	18	(c	(c	PROPN
eurjchem-376	53	19	=	=	SYM
eurjchem-376	53	20	n	n	NUM
eurjchem-376	53	21	)	)	PUNCT
eurjchem-376	53	22	,	,	PUNCT
eurjchem-376	53	23	1635	1635	NUM
eurjchem-376	53	24	(c	(c	PROPN
eurjchem-376	53	25	=	=	SYM
eurjchem-376	53	26	c	c	NOUN
eurjchem-376	53	27	)	)	PUNCT
eurjchem-376	53	28	.	.	PUNCT
eurjchem-376	54	1	1h	1h	NUM
eurjchem-376	54	2	nmr	nmr	NOUN
eurjchem-376	54	3	(	(	PUNCT
eurjchem-376	54	4	200	200	NUM
eurjchem-376	54	5	mhz	mhz	NOUN
eurjchem-376	54	6	,	,	PUNCT
eurjchem-376	54	7	cdcl3	cdcl3	NOUN
eurjchem-376	54	8	):	):	PUNCT
eurjchem-376	54	9	8.52	8.52	NUM
eurjchem-376	54	10	,	,	PUNCT
eurjchem-376	54	11	9.33	9.33	NUM
eurjchem-376	54	12	(	(	PUNCT
eurjchem-376	54	13	2s	2s	NUM
eurjchem-376	54	14	,	,	PUNCT
eurjchem-376	54	15	2h	2h	NUM
eurjchem-376	54	16	,	,	PUNCT
eurjchem-376	54	17	2nh	2nh	NOUN
eurjchem-376	54	18	,	,	PUNCT
eurjchem-376	54	19	exchangeable	exchangeable	ADJ
eurjchem-376	54	20	)	)	PUNCT
eurjchem-376	54	21	,	,	PUNCT
eurjchem-376	54	22	10.24	10.24	NUM
eurjchem-376	54	23	(	(	PUNCT
eurjchem-376	54	24	s	s	PROPN
eurjchem-376	54	25	,	,	PUNCT
eurjchem-376	54	26	1h	1h	NUM
eurjchem-376	54	27	,	,	PUNCT
eurjchem-376	54	28	oh	oh	INTJ
eurjchem-376	54	29	)	)	PUNCT
eurjchem-376	54	30	,	,	PUNCT
eurjchem-376	54	31	7.02‐7.98	7.02‐7.98	NUM
eurjchem-376	54	32	(	(	PUNCT
eurjchem-376	54	33	m	m	PROPN
eurjchem-376	54	34	,	,	PUNCT
eurjchem-376	54	35	14h	14h	NUM
eurjchem-376	54	36	,	,	PUNCT
eurjchem-376	54	37	ar‐h	ar‐h	NOUN
eurjchem-376	54	38	)	)	PUNCT
eurjchem-376	54	39	.	.	PUNCT
eurjchem-376	55	1	ms	ms	NOUN
eurjchem-376	55	2	(	(	PUNCT
eurjchem-376	55	3	m	m	PROPN
eurjchem-376	55	4	/	/	SYM
eurjchem-376	55	5	z	z	NOUN
eurjchem-376	55	6	):	):	PUNCT
eurjchem-376	55	7	463	463	NUM
eurjchem-376	55	8	(	(	PUNCT
eurjchem-376	55	9	m+	m+	NUM
eurjchem-376	55	10	)	)	PUNCT
eurjchem-376	55	11	.	.	PUNCT
eurjchem-376	56	1	anal	anal	PROPN
eurjchem-376	56	2	.	.	PUNCT
eurjchem-376	56	3	calcd	calcd	NOUN
eurjchem-376	56	4	.	.	PUNCT
eurjchem-376	57	1	for	for	ADP
eurjchem-376	57	2	c26h17n5o2s	c26h17n5o2s	NUM
eurjchem-376	57	3	:	:	PUNCT
eurjchem-376	57	4	c	c	X
eurjchem-376	57	5	,	,	PUNCT
eurjchem-376	57	6	67.37	67.37	NUM
eurjchem-376	57	7	;	;	PUNCT
eurjchem-376	57	8	h	h	NOUN
eurjchem-376	57	9	,	,	PUNCT
eurjchem-376	57	10	3.70	3.70	NUM
eurjchem-376	57	11	;	;	PUNCT
eurjchem-376	57	12	n	n	CCONJ
eurjchem-376	57	13	,	,	PUNCT
eurjchem-376	57	14	15.11	15.11	NUM
eurjchem-376	57	15	.	.	PUNCT
eurjchem-376	57	16	found	find	VERB
eurjchem-376	57	17	:	:	PUNCT
eurjchem-376	58	1	c	c	X
eurjchem-376	58	2	,	,	PUNCT
eurjchem-376	58	3	67.20	67.20	NUM
eurjchem-376	58	4	;	;	PUNCT
eurjchem-376	58	5	h	h	NOUN
eurjchem-376	58	6	,	,	PUNCT
eurjchem-376	58	7	3.53	3.53	NUM
eurjchem-376	58	8	;	;	PUNCT
eurjchem-376	58	9	n	n	CCONJ
eurjchem-376	58	10	,	,	PUNCT
eurjchem-376	58	11	14.85	14.85	NUM
eurjchem-376	58	12	%	%	NOUN
eurjchem-376	58	13	.	.	PUNCT
eurjchem-376	59	1	n‐(6‐dibenzothiophen‐2‐yl	n‐(6‐dibenzothiophen‐2‐yl	PROPN
eurjchem-376	59	2	–	–	PUNCT
eurjchem-376	59	3	pyridazin‐3‐yl)‐3‐hydroxy‐1,5‐	pyridazin‐3‐yl)‐3‐hydroxy‐1,5‐	PROPN
eurjchem-376	59	4	diphenyl‐1h‐pyrazole‐4‐carboxamide	diphenyl‐1h‐pyrazole‐4‐carboxamide	ADP
eurjchem-376	59	5	(	(	PUNCT
eurjchem-376	59	6	4b	4b	X
eurjchem-376	59	7	):	):	PUNCT
eurjchem-376	59	8	yellow	yellow	ADJ
eurjchem-376	59	9	,	,	PUNCT
eurjchem-376	59	10	yield	yield	NOUN
eurjchem-376	59	11	:	:	PUNCT
eurjchem-376	59	12	74	74	NUM
eurjchem-376	59	13	%	%	NOUN
eurjchem-376	59	14	(	(	PUNCT
eurjchem-376	59	15	ethanol	ethanol	NOUN
eurjchem-376	59	16	)	)	PUNCT
eurjchem-376	59	17	.	.	PUNCT
eurjchem-376	60	1	m.p	m.p	PROPN
eurjchem-376	60	2	.	.	PROPN
eurjchem-376	60	3	:	:	PUNCT
eurjchem-376	61	1	186‐188	186‐188	NUM
eurjchem-376	61	2	c	c	ADJ
eurjchem-376	61	3	.	.	PUNCT
eurjchem-376	62	1	ir	ir	PROPN
eurjchem-376	62	2	(	(	PUNCT
eurjchem-376	62	3	kbr	kbr	PROPN
eurjchem-376	62	4	,	,	PUNCT
eurjchem-376	62	5	cm‐1	cm‐1	PROPN
eurjchem-376	62	6	):	):	PUNCT
eurjchem-376	62	7	3460‐3255	3460‐3255	NUM
eurjchem-376	62	8	(oh	(oh	NOUN
eurjchem-376	62	9	,	,	PUNCT
eurjchem-376	62	10	nh	nh	PROPN
eurjchem-376	62	11	)	)	PUNCT
eurjchem-376	62	12	,	,	PUNCT
eurjchem-376	62	13	1685	1685	NUM
eurjchem-376	62	14	(co	(co	NOUN
eurjchem-376	62	15	)	)	PUNCT
eurjchem-376	62	16	,	,	PUNCT
eurjchem-376	62	17	1645	1645	NUM
eurjchem-376	62	18	(c	(c	PROPN
eurjchem-376	62	19	=	=	SYM
eurjchem-376	62	20	n	n	NUM
eurjchem-376	62	21	)	)	PUNCT
eurjchem-376	62	22	,	,	PUNCT
eurjchem-376	62	23	1622	1622	NUM
eurjchem-376	62	24	(c	(c	PROPN
eurjchem-376	62	25	=	=	SYM
eurjchem-376	62	26	c	c	NOUN
eurjchem-376	62	27	)	)	PUNCT
eurjchem-376	62	28	.	.	PUNCT
eurjchem-376	63	1	1h	1h	NUM
eurjchem-376	63	2	nmr	nmr	NOUN
eurjchem-376	63	3	(	(	PUNCT
eurjchem-376	63	4	200	200	NUM
eurjchem-376	63	5	mhz	mhz	NOUN
eurjchem-376	63	6	,	,	PUNCT
eurjchem-376	63	7	cdcl3	cdcl3	NOUN
eurjchem-376	63	8	):	):	PUNCT
eurjchem-376	63	9	8.90	8.90	NUM
eurjchem-376	63	10	(	(	PUNCT
eurjchem-376	63	11	s	s	PROPN
eurjchem-376	63	12	,	,	PUNCT
eurjchem-376	63	13	1h	1h	NUM
eurjchem-376	63	14	,	,	PUNCT
eurjchem-376	63	15	nh	nh	PROPN
eurjchem-376	63	16	,	,	PUNCT
eurjchem-376	63	17	exchangeable	exchangeable	ADJ
eurjchem-376	63	18	)	)	PUNCT
eurjchem-376	63	19	,	,	PUNCT
eurjchem-376	63	20	10.28	10.28	NUM
eurjchem-376	63	21	(	(	PUNCT
eurjchem-376	63	22	s	s	PROPN
eurjchem-376	63	23	,	,	PUNCT
eurjchem-376	63	24	1h	1h	NUM
eurjchem-376	63	25	,	,	PUNCT
eurjchem-376	63	26	oh	oh	INTJ
eurjchem-376	63	27	)	)	PUNCT
eurjchem-376	63	28	,	,	PUNCT
eurjchem-376	63	29	7.89‐8.10	7.89‐8.10	NUM
eurjchem-376	63	30	(	(	PUNCT
eurjchem-376	63	31	m	m	PROPN
eurjchem-376	63	32	,	,	PUNCT
eurjchem-376	63	33	h	h	NOUN
eurjchem-376	63	34	,	,	PUNCT
eurjchem-376	63	35	19ar‐h	19ar‐h	PROPN
eurjchem-376	63	36	)	)	PUNCT
eurjchem-376	63	37	.	.	PUNCT
eurjchem-376	64	1	ms	ms	NOUN
eurjchem-376	64	2	(	(	PUNCT
eurjchem-376	64	3	m	m	PROPN
eurjchem-376	64	4	/	/	SYM
eurjchem-376	64	5	z	z	NOUN
eurjchem-376	64	6	):	):	PUNCT
eurjchem-376	64	7	539	539	NUM
eurjchem-376	64	8	(	(	PUNCT
eurjchem-376	64	9	m+	m+	NUM
eurjchem-376	64	10	)	)	PUNCT
eurjchem-376	64	11	.	.	PUNCT
eurjchem-376	65	1	anal	anal	PROPN
eurjchem-376	65	2	.	.	PUNCT
eurjchem-376	65	3	calcd	calcd	NOUN
eurjchem-376	65	4	.	.	PUNCT
eurjchem-376	66	1	for	for	SCONJ
eurjchem-376	66	2	c32h21n5o2s	c32h21n5o2s	NOUN
eurjchem-376	66	3	:	:	PUNCT
eurjchem-376	66	4	c	c	X
eurjchem-376	66	5	,	,	PUNCT
eurjchem-376	66	6	71.23	71.23	NUM
eurjchem-376	66	7	;	;	PUNCT
eurjchem-376	66	8	h	h	NOUN
eurjchem-376	66	9	,	,	PUNCT
eurjchem-376	66	10	3.92	3.92	NUM
eurjchem-376	66	11	;	;	PUNCT
eurjchem-376	66	12	n	n	CCONJ
eurjchem-376	66	13	,	,	PUNCT
eurjchem-376	66	14	12.98	12.98	NUM
eurjchem-376	66	15	.	.	PUNCT
eurjchem-376	66	16	found	find	VERB
eurjchem-376	66	17	:	:	PUNCT
eurjchem-376	67	1	c	c	X
eurjchem-376	67	2	,	,	PUNCT
eurjchem-376	67	3	71.04	71.04	NUM
eurjchem-376	67	4	;	;	PUNCT
eurjchem-376	67	5	h	h	NOUN
eurjchem-376	67	6	,	,	PUNCT
eurjchem-376	67	7	3.64	3.64	NUM
eurjchem-376	67	8	;	;	PUNCT
eurjchem-376	67	9	n	n	CCONJ
eurjchem-376	67	10	,	,	PUNCT
eurjchem-376	67	11	12.74	12.74	NUM
eurjchem-376	67	12	%	%	NOUN
eurjchem-376	67	13	.	.	PUNCT
eurjchem-376	68	1	2.1.4	2.1.4	NUM
eurjchem-376	68	2	.	.	PUNCT
eurjchem-376	68	3	n‐(6‐dibenzothiophen‐2‐yl	n‐(6‐dibenzothiophen‐2‐yl	PROPN
eurjchem-376	68	4	–	–	PUNCT
eurjchem-376	68	5	pyridazin‐3‐yl)‐2‐oxo‐2h‐	pyridazin‐3‐yl)‐2‐oxo‐2h‐	NOUN
eurjchem-376	68	6	chromene‐3‐carbox	chromene‐3‐carbox	NOUN
eurjchem-376	68	7	amide	amide	NOUN
eurjchem-376	68	8	(	(	PUNCT
eurjchem-376	68	9	5	5	NUM
eurjchem-376	68	10	)	)	PUNCT
eurjchem-376	68	11	the	the	DET
eurjchem-376	68	12	same	same	ADJ
eurjchem-376	68	13	procedures	procedure	NOUN
eurjchem-376	68	14	described	describe	VERB
eurjchem-376	68	15	for	for	ADP
eurjchem-376	68	16	the	the	DET
eurjchem-376	68	17	synthesis	synthesis	NOUN
eurjchem-376	68	18	of	of	ADP
eurjchem-376	68	19	compound	compound	NOUN
eurjchem-376	68	20	3	3	NUM
eurjchem-376	68	21	.	.	PUNCT
eurjchem-376	68	22	yellow	yellow	ADJ
eurjchem-376	68	23	,	,	PUNCT
eurjchem-376	68	24	yield	yield	NOUN
eurjchem-376	68	25	:	:	PUNCT
eurjchem-376	68	26	82	82	NUM
eurjchem-376	68	27	%	%	NOUN
eurjchem-376	68	28	(	(	PUNCT
eurjchem-376	68	29	ethanol	ethanol	NOUN
eurjchem-376	68	30	)	)	PUNCT
eurjchem-376	68	31	(	(	PUNCT
eurjchem-376	68	32	scheme	scheme	NOUN
eurjchem-376	68	33	2	2	NUM
eurjchem-376	68	34	)	)	PUNCT
eurjchem-376	68	35	.	.	PUNCT
eurjchem-376	69	1	m.p	m.p	PROPN
eurjchem-376	69	2	.	.	PROPN
eurjchem-376	69	3	206‐208	206‐208	NUM
eurjchem-376	69	4	c	c	ADJ
eurjchem-376	69	5	.	.	PUNCT
eurjchem-376	70	1	ir	ir	PROPN
eurjchem-376	70	2	(	(	PUNCT
eurjchem-376	70	3	kbr	kbr	PROPN
eurjchem-376	70	4	,	,	PUNCT
eurjchem-376	70	5	cm‐1	cm‐1	PROPN
eurjchem-376	70	6	):	):	PUNCT
eurjchem-376	70	7	3390‐3270	3390‐3270	NUM
eurjchem-376	70	8	(nh	(nh	NOUN
eurjchem-376	70	9	)	)	PUNCT
eurjchem-376	70	10	,	,	PUNCT
eurjchem-376	70	11	3020	3020	NUM
eurjchem-376	70	12	(ch‐	(ch‐	DET
eurjchem-376	70	13	aromatic	aromatic	NOUN
eurjchem-376	70	14	)	)	PUNCT
eurjchem-376	70	15	,	,	PUNCT
eurjchem-376	70	16	1710	1710	NUM
eurjchem-376	70	17	,	,	PUNCT
eurjchem-376	70	18	1680	1680	NUM
eurjchem-376	70	19	(co	(co	NOUN
eurjchem-376	70	20	)	)	PUNCT
eurjchem-376	70	21	,	,	PUNCT
eurjchem-376	70	22	1620	1620	NUM
eurjchem-376	70	23	(c	(c	PROPN
eurjchem-376	70	24	=	=	SYM
eurjchem-376	70	25	c	c	NOUN
eurjchem-376	70	26	)	)	PUNCT
eurjchem-376	70	27	.	.	PUNCT
eurjchem-376	71	1	1h	1h	NUM
eurjchem-376	71	2	nmr	nmr	NOUN
eurjchem-376	71	3	(	(	PUNCT
eurjchem-376	71	4	200	200	NUM
eurjchem-376	71	5	mhz	mhz	NOUN
eurjchem-376	71	6	,	,	PUNCT
eurjchem-376	71	7	cdcl3	cdcl3	NOUN
eurjchem-376	71	8	):	):	PUNCT
eurjchem-376	71	9	6.92‐7.88	6.92‐7.88	NUM
eurjchem-376	71	10	(	(	PUNCT
eurjchem-376	71	11	m	m	PROPN
eurjchem-376	71	12	,	,	PUNCT
eurjchem-376	71	13	14h	14h	NUM
eurjchem-376	71	14	,	,	PUNCT
eurjchem-376	71	15	arh+chromene‐h	arh+chromene‐h	PROPN
eurjchem-376	71	16	)	)	PUNCT
eurjchem-376	71	17	,	,	PUNCT
eurjchem-376	71	18	8.93	8.93	NUM
eurjchem-376	71	19	(	(	PUNCT
eurjchem-376	71	20	s	s	PROPN
eurjchem-376	71	21	,	,	PUNCT
eurjchem-376	71	22	1h	1h	NUM
eurjchem-376	71	23	,	,	PUNCT
eurjchem-376	71	24	nh	nh	PROPN
eurjchem-376	71	25	,	,	PUNCT
eurjchem-376	71	26	exchangeable	exchangeable	ADJ
eurjchem-376	71	27	)	)	PUNCT
eurjchem-376	71	28	.	.	PUNCT
eurjchem-376	72	1	13	13	NUM
eurjchem-376	72	2	c	c	PROPN
eurjchem-376	72	3	nmr	nmr	NOUN
eurjchem-376	72	4	(	(	PUNCT
eurjchem-376	72	5	50	50	NUM
eurjchem-376	72	6	mhz	mhz	NOUN
eurjchem-376	72	7	,	,	PUNCT
eurjchem-376	72	8	cdcl3	cdcl3	NOUN
eurjchem-376	72	9	):	):	PUNCT
eurjchem-376	72	10	120.2	120.2	NUM
eurjchem-376	72	11	,	,	PUNCT
eurjchem-376	72	12	123.6	123.6	NUM
eurjchem-376	72	13	,	,	PUNCT
eurjchem-376	72	14	126.1	126.1	NUM
eurjchem-376	72	15	,	,	PUNCT
eurjchem-376	72	16	126.9	126.9	NUM
eurjchem-376	72	17	,	,	PUNCT
eurjchem-376	72	18	127.5	127.5	NUM
eurjchem-376	72	19	,	,	PUNCT
eurjchem-376	72	20	128.6	128.6	NUM
eurjchem-376	72	21	,	,	PUNCT
eurjchem-376	72	22	148.3	148.3	NUM
eurjchem-376	72	23	,	,	PUNCT
eurjchem-376	72	24	150.2	150.2	NUM
eurjchem-376	72	25	,	,	PUNCT
eurjchem-376	72	26	(	(	PUNCT
eurjchem-376	72	27	in	in	ADP
eurjchem-376	72	28	addition	addition	NOUN
eurjchem-376	72	29	to	to	ADP
eurjchem-376	72	30	dibenzo	dibenzo	NOUN
eurjchem-376	72	31	thiophene	thiophene	NOUN
eurjchem-376	72	32	and	and	CCONJ
eurjchem-376	72	33	pyridazine	pyridazine	NOUN
eurjchem-376	72	34	carbons	carbon	NOUN
eurjchem-376	72	35	)	)	PUNCT
eurjchem-376	72	36	,	,	PUNCT
eurjchem-376	72	37	162.2	162.2	NUM
eurjchem-376	72	38	,	,	PUNCT
eurjchem-376	72	39	163.4	163.4	NUM
eurjchem-376	72	40	(	(	PUNCT
eurjchem-376	72	41	2co	2co	NOUN
eurjchem-376	72	42	)	)	PUNCT
eurjchem-376	72	43	.	.	PUNCT
eurjchem-376	73	1	ms	ms	NOUN
eurjchem-376	73	2	(	(	PUNCT
eurjchem-376	73	3	m	m	PROPN
eurjchem-376	73	4	/	/	SYM
eurjchem-376	73	5	z	z	NOUN
eurjchem-376	73	6	):	):	PUNCT
eurjchem-376	73	7	449	449	NUM
eurjchem-376	73	8	(	(	PUNCT
eurjchem-376	73	9	m+	m+	NUM
eurjchem-376	73	10	)	)	PUNCT
eurjchem-376	73	11	;	;	PUNCT
eurjchem-376	73	12	anal	anal	ADJ
eurjchem-376	73	13	.	.	PUNCT
eurjchem-376	73	14	calcd	calcd	NOUN
eurjchem-376	73	15	.	.	PUNCT
eurjchem-376	74	1	for	for	SCONJ
eurjchem-376	74	2	c26h15n3o3s	c26h15n3o3s	NUM
eurjchem-376	74	3	:	:	PUNCT
eurjchem-376	74	4	c	c	X
eurjchem-376	74	5	,	,	PUNCT
eurjchem-376	74	6	69.48	69.48	NUM
eurjchem-376	74	7	;	;	PUNCT
eurjchem-376	74	8	h	h	NOUN
eurjchem-376	74	9	,	,	PUNCT
eurjchem-376	74	10	3.36	3.36	NUM
eurjchem-376	74	11	;	;	PUNCT
eurjchem-376	74	12	n	n	CCONJ
eurjchem-376	74	13	,	,	PUNCT
eurjchem-376	74	14	9.35	9.35	NUM
eurjchem-376	74	15	.	.	PUNCT
eurjchem-376	74	16	found	find	VERB
eurjchem-376	74	17	:	:	PUNCT
eurjchem-376	75	1	c	c	X
eurjchem-376	75	2	,	,	PUNCT
eurjchem-376	75	3	69.25	69.25	NUM
eurjchem-376	75	4	;	;	PUNCT
eurjchem-376	75	5	h	h	NOUN
eurjchem-376	75	6	,	,	PUNCT
eurjchem-376	75	7	3.16	3.16	NUM
eurjchem-376	75	8	;	;	PUNCT
eurjchem-376	75	9	n	n	CCONJ
eurjchem-376	75	10	,	,	PUNCT
eurjchem-376	75	11	9.18	9.18	NUM
eurjchem-376	75	12	%	%	NOUN
eurjchem-376	75	13	.	.	PUNCT
eurjchem-376	76	1	2.1.5	2.1.5	NUM
eurjchem-376	76	2	.	.	PUNCT
eurjchem-376	76	3	ethyl	ethyl	PROPN
eurjchem-376	76	4	3‐(6‐dibenzothiophen‐2‐yl	3‐(6‐dibenzothiophen‐2‐yl	NUM
eurjchem-376	76	5	–	–	PUNCT
eurjchem-376	76	6	pyridazin‐3‐	pyridazin‐3‐	NUM
eurjchem-376	76	7	ylamino)‐3‐oxo‐2‐(phenylhyda	ylamino)‐3‐oxo‐2‐(phenylhyda	ADJ
eurjchem-376	76	8	zono)propanoate	zono)propanoate	NOUN
eurjchem-376	76	9	(	(	PUNCT
eurjchem-376	76	10	6	6	NUM
eurjchem-376	76	11	)	)	PUNCT
eurjchem-376	76	12	a	a	DET
eurjchem-376	76	13	cold	cold	ADJ
eurjchem-376	76	14	solution	solution	NOUN
eurjchem-376	76	15	of	of	ADP
eurjchem-376	76	16	benzene	benzene	NOUN
eurjchem-376	76	17	diazonium	diazonium	NOUN
eurjchem-376	76	18	chloride	chloride	NOUN
eurjchem-376	76	19	(	(	PUNCT
eurjchem-376	76	20	0.01	0.01	NUM
eurjchem-376	76	21	mol	mol	NOUN
eurjchem-376	76	22	)	)	PUNCT
eurjchem-376	76	23	was	be	AUX
eurjchem-376	76	24	added	add	VERB
eurjchem-376	76	25	to	to	ADP
eurjchem-376	76	26	stirred	stir	VERB
eurjchem-376	76	27	solution	solution	NOUN
eurjchem-376	76	28	of	of	ADP
eurjchem-376	76	29	3	3	NUM
eurjchem-376	76	30	(	(	PUNCT
eurjchem-376	76	31	0.01	0.01	NUM
eurjchem-376	76	32	mol	mol	NOUN
eurjchem-376	76	33	)	)	PUNCT
eurjchem-376	76	34	in	in	ADP
eurjchem-376	76	35	ethanol	ethanol	NOUN
eurjchem-376	76	36	(	(	PUNCT
eurjchem-376	76	37	30	30	NUM
eurjchem-376	76	38	ml	ml	NOUN
eurjchem-376	76	39	)	)	PUNCT
eurjchem-376	76	40	.	.	PUNCT
eurjchem-376	77	1	the	the	DET
eurjchem-376	77	2	reaction	reaction	NOUN
eurjchem-376	77	3	mixture	mixture	NOUN
eurjchem-376	77	4	was	be	AUX
eurjchem-376	77	5	stirred	stir	VERB
eurjchem-376	77	6	at	at	ADP
eurjchem-376	77	7	room	room	NOUN
eurjchem-376	77	8	temperature	temperature	NOUN
eurjchem-376	77	9	for	for	ADP
eurjchem-376	77	10	3	3	NUM
eurjchem-376	77	11	hours	hour	NOUN
eurjchem-376	77	12	and	and	CCONJ
eurjchem-376	77	13	the	the	DET
eurjchem-376	77	14	formed	form	VERB
eurjchem-376	77	15	solid	solid	ADJ
eurjchem-376	77	16	product	product	NOUN
eurjchem-376	77	17	was	be	AUX
eurjchem-376	77	18	collected	collect	VERB
eurjchem-376	77	19	by	by	ADP
eurjchem-376	77	20	filtration	filtration	NOUN
eurjchem-376	77	21	and	and	CCONJ
eurjchem-376	77	22	washed	wash	VERB
eurjchem-376	77	23	:	:	PUNCT
eurjchem-376	77	24	orange	orange	ADJ
eurjchem-376	77	25	,	,	PUNCT
eurjchem-376	77	26	yield	yield	NOUN
eurjchem-376	77	27	:	:	PUNCT
eurjchem-376	77	28	78	78	NUM
eurjchem-376	77	29	%	%	NOUN
eurjchem-376	77	30	(	(	PUNCT
eurjchem-376	77	31	ethanol	ethanol	NOUN
eurjchem-376	77	32	)	)	PUNCT
eurjchem-376	77	33	(	(	PUNCT
eurjchem-376	77	34	scheme	scheme	NOUN
eurjchem-376	77	35	2	2	NUM
eurjchem-376	77	36	)	)	PUNCT
eurjchem-376	77	37	.	.	PUNCT
eurjchem-376	78	1	m.p	m.p	PROPN
eurjchem-376	78	2	.	.	PROPN
eurjchem-376	78	3	:	:	PUNCT
eurjchem-376	78	4	170‐172	170‐172	PROPN
eurjchem-376	78	5	c	c	VERB
eurjchem-376	78	6	.	.	PUNCT
eurjchem-376	79	1	ir	ir	PROPN
eurjchem-376	79	2	(	(	PUNCT
eurjchem-376	79	3	kbr	kbr	PROPN
eurjchem-376	79	4	,	,	PUNCT
eurjchem-376	79	5	cm‐1	cm‐1	PROPN
eurjchem-376	79	6	):	):	PUNCT
eurjchem-376	79	7	2930	2930	NUM
eurjchem-376	79	8	,	,	PUNCT
eurjchem-376	79	9	2850	2850	NUM
eurjchem-376	79	10	(ch‐aliphatic	(ch‐aliphatic	NOUN
eurjchem-376	79	11	)	)	PUNCT
eurjchem-376	79	12	,	,	PUNCT
eurjchem-376	79	13	1705	1705	NUM
eurjchem-376	79	14	,	,	PUNCT
eurjchem-376	79	15	1685	1685	NUM
eurjchem-376	79	16	(co	(co	NOUN
eurjchem-376	79	17	)	)	PUNCT
eurjchem-376	79	18	,	,	PUNCT
eurjchem-376	79	19	3360‐3225	3360‐3225	NUM
eurjchem-376	79	20	(nh	(nh	PROPN
eurjchem-376	79	21	)	)	PUNCT
eurjchem-376	79	22	.	.	PUNCT
eurjchem-376	80	1	1h	1h	NUM
eurjchem-376	80	2	nmr	nmr	NOUN
eurjchem-376	80	3	(	(	PUNCT
eurjchem-376	80	4	200	200	NUM
eurjchem-376	80	5	mhz	mhz	NOUN
eurjchem-376	80	6	,	,	PUNCT
eurjchem-376	80	7	cdcl3	cdcl3	NOUN
eurjchem-376	80	8	):	):	PUNCT
eurjchem-376	80	9	1.32	1.32	NUM
eurjchem-376	80	10	(	(	PUNCT
eurjchem-376	80	11	t	t	PROPN
eurjchem-376	80	12	,	,	PUNCT
eurjchem-376	80	13	3	3	NUM
eurjchem-376	80	14	h	h	NOUN
eurjchem-376	80	15	,	,	PUNCT
eurjchem-376	80	16	ch3	ch3	PROPN
eurjchem-376	80	17	)	)	PUNCT
eurjchem-376	80	18	,	,	PUNCT
eurjchem-376	80	19	4.21	4.21	NUM
eurjchem-376	80	20	(	(	PUNCT
eurjchem-376	80	21	q	q	NOUN
eurjchem-376	80	22	,	,	PUNCT
eurjchem-376	80	23	2h	2h	NUM
eurjchem-376	80	24	,	,	PUNCT
eurjchem-376	80	25	ch2	ch2	PROPN
eurjchem-376	80	26	)	)	PUNCT
eurjchem-376	80	27	,	,	PUNCT
eurjchem-376	80	28	6.83‐8.02	6.83‐8.02	NUM
eurjchem-376	80	29	(	(	PUNCT
eurjchem-376	80	30	m	m	PROPN
eurjchem-376	80	31	,	,	PUNCT
eurjchem-376	80	32	14h	14h	NUM
eurjchem-376	80	33	,	,	PUNCT
eurjchem-376	80	34	arh	arh	PROPN
eurjchem-376	80	35	)	)	PUNCT
eurjchem-376	80	36	,	,	PUNCT
eurjchem-376	80	37	8.84	8.84	NUM
eurjchem-376	80	38	,	,	PUNCT
eurjchem-376	80	39	9.23	9.23	NUM
eurjchem-376	80	40	(	(	PUNCT
eurjchem-376	80	41	2s	2s	NUM
eurjchem-376	80	42	,	,	PUNCT
eurjchem-376	80	43	2h	2h	NUM
eurjchem-376	80	44	,	,	PUNCT
eurjchem-376	80	45	2nh	2nh	NOUN
eurjchem-376	80	46	,	,	PUNCT
eurjchem-376	80	47	exchangeable	exchangeable	ADJ
eurjchem-376	80	48	)	)	PUNCT
eurjchem-376	80	49	.	.	PUNCT
eurjchem-376	81	1	ms	ms	NOUN
eurjchem-376	81	2	(	(	PUNCT
eurjchem-376	81	3	m	m	PROPN
eurjchem-376	81	4	/	/	SYM
eurjchem-376	81	5	z	z	NOUN
eurjchem-376	81	6	):	):	PUNCT
eurjchem-376	81	7	495	495	NUM
eurjchem-376	81	8	(	(	PUNCT
eurjchem-376	81	9	m+	m+	NUM
eurjchem-376	81	10	)	)	PUNCT
eurjchem-376	81	11	.	.	PUNCT
eurjchem-376	82	1	anal	anal	PROPN
eurjchem-376	82	2	.	.	PUNCT
eurjchem-376	82	3	calcd	calcd	NOUN
eurjchem-376	82	4	.	.	PUNCT
eurjchem-376	83	1	for	for	ADP
eurjchem-376	83	2	c27h21n5o3s	c27h21n5o3s	NUM
eurjchem-376	83	3	:	:	PUNCT
eurjchem-376	83	4	c	c	X
eurjchem-376	83	5	,	,	PUNCT
eurjchem-376	83	6	65.44	65.44	NUM
eurjchem-376	83	7	;	;	PUNCT
eurjchem-376	83	8	h	h	X
eurjchem-376	83	9	,	,	PUNCT
eurjchem-376	83	10	4.27	4.27	NUM
eurjchem-376	83	11	;	;	PUNCT
eurjchem-376	83	12	n	n	CCONJ
eurjchem-376	83	13	,	,	PUNCT
eurjchem-376	83	14	14.13	14.13	NUM
eurjchem-376	83	15	.	.	PUNCT
eurjchem-376	83	16	found	find	VERB
eurjchem-376	83	17	:	:	PUNCT
eurjchem-376	84	1	c	c	X
eurjchem-376	84	2	,	,	PUNCT
eurjchem-376	84	3	65.32	65.32	NUM
eurjchem-376	84	4	;	;	PUNCT
eurjchem-376	84	5	h	h	NOUN
eurjchem-376	84	6	,	,	PUNCT
eurjchem-376	84	7	4.07	4.07	NUM
eurjchem-376	84	8	;	;	PUNCT
eurjchem-376	84	9	n	n	CCONJ
eurjchem-376	84	10	,	,	PUNCT
eurjchem-376	84	11	13.94	13.94	NUM
eurjchem-376	84	12	%	%	NOUN
eurjchem-376	84	13	.	.	PUNCT
eurjchem-376	85	1	2.1.6	2.1.6	X
eurjchem-376	85	2	.	.	PUNCT
eurjchem-376	85	3	n‐(6‐dibenzothiophen‐2‐yl	n‐(6‐dibenzothiophen‐2‐yl	PROPN
eurjchem-376	85	4	–	–	PUNCT
eurjchem-376	85	5	pyridazin‐3‐yl)‐5‐hydroxy‐	pyridazin‐3‐yl)‐5‐hydroxy‐	NOUN
eurjchem-376	85	6	2‐phenyl‐2h‐1,2,3‐triazole‐4‐	2‐phenyl‐2h‐1,2,3‐triazole‐4‐	NUM
eurjchem-376	85	7	carboxamide	carboxamide	NOUN
eurjchem-376	85	8	(	(	PUNCT
eurjchem-376	85	9	7	7	NUM
eurjchem-376	85	10	)	)	PUNCT
eurjchem-376	85	11	a	a	DET
eurjchem-376	85	12	mixture	mixture	NOUN
eurjchem-376	85	13	of	of	ADP
eurjchem-376	85	14	hydrazone	hydrazone	NOUN
eurjchem-376	85	15	6	6	NUM
eurjchem-376	85	16	(	(	PUNCT
eurjchem-376	85	17	0.01	0.01	NUM
eurjchem-376	85	18	mol	mol	NOUN
eurjchem-376	85	19	)	)	PUNCT
eurjchem-376	85	20	and	and	CCONJ
eurjchem-376	85	21	hydrazine	hydrazine	NOUN
eurjchem-376	85	22	hydrate	hydrate	NOUN
eurjchem-376	85	23	(	(	PUNCT
eurjchem-376	85	24	0.01	0.01	NUM
eurjchem-376	85	25	mol	mol	NOUN
eurjchem-376	85	26	)	)	PUNCT
eurjchem-376	85	27	in	in	ADP
eurjchem-376	85	28	ethanol	ethanol	NOUN
eurjchem-376	85	29	(	(	PUNCT
eurjchem-376	85	30	30	30	NUM
eurjchem-376	85	31	ml	ml	NOUN
eurjchem-376	85	32	)	)	PUNCT
eurjchem-376	85	33	was	be	AUX
eurjchem-376	85	34	heated	heat	VERB
eurjchem-376	85	35	under	under	ADP
eurjchem-376	85	36	reflux	reflux	NOUN
eurjchem-376	85	37	for	for	ADP
eurjchem-376	85	38	4	4	NUM
eurjchem-376	85	39	hours	hour	NOUN
eurjchem-376	85	40	.	.	PUNCT
eurjchem-376	86	1	after	after	ADP
eurjchem-376	86	2	evaporation	evaporation	NOUN
eurjchem-376	86	3	of	of	ADP
eurjchem-376	86	4	solvent	solvent	NOUN
eurjchem-376	86	5	on	on	ADP
eurjchem-376	86	6	a	a	DET
eurjchem-376	86	7	vacuum	vacuum	NOUN
eurjchem-376	86	8	,	,	PUNCT
eurjchem-376	86	9	the	the	DET
eurjchem-376	86	10	solid	solid	ADJ
eurjchem-376	86	11	product	product	NOUN
eurjchem-376	86	12	was	be	AUX
eurjchem-376	86	13	recrystallized	recrystallize	VERB
eurjchem-376	86	14	:	:	PUNCT
eurjchem-376	86	15	yellow	yellow	ADJ
eurjchem-376	86	16	,	,	PUNCT
eurjchem-376	86	17	yield	yield	VERB
eurjchem-376	86	18	70	70	NUM
eurjchem-376	86	19	%	%	NOUN
eurjchem-376	86	20	(	(	PUNCT
eurjchem-376	86	21	acetone	acetone	NOUN
eurjchem-376	86	22	)	)	PUNCT
eurjchem-376	86	23	(	(	PUNCT
eurjchem-376	86	24	scheme	scheme	NOUN
eurjchem-376	86	25	2	2	NUM
eurjchem-376	86	26	)	)	PUNCT
eurjchem-376	86	27	.	.	PUNCT
eurjchem-376	87	1	m.p	m.p	PROPN
eurjchem-376	87	2	.	.	PROPN
eurjchem-376	87	3	:	:	PUNCT
eurjchem-376	88	1	180‐182	180‐182	PROPN
eurjchem-376	88	2	c	c	ADJ
eurjchem-376	88	3	.	.	PUNCT
eurjchem-376	89	1	ir	ir	PROPN
eurjchem-376	89	2	(	(	PUNCT
eurjchem-376	89	3	kbr	kbr	PROPN
eurjchem-376	89	4	,	,	PUNCT
eurjchem-376	89	5	cm‐1	cm‐1	PROPN
eurjchem-376	89	6	):	):	PUNCT
eurjchem-376	89	7	3480‐3255	3480‐3255	NUM
eurjchem-376	89	8	(oh	(oh	NOUN
eurjchem-376	89	9	,	,	PUNCT
eurjchem-376	89	10	nh	nh	PROPN
eurjchem-376	89	11	)	)	PUNCT
eurjchem-376	89	12	,	,	PUNCT
eurjchem-376	89	13	1680	1680	NUM
eurjchem-376	89	14	(co	(co	NOUN
eurjchem-376	89	15	)	)	PUNCT
eurjchem-376	89	16	,	,	PUNCT
eurjchem-376	89	17	1630	1630	NUM
eurjchem-376	89	18	(c	(c	PROPN
eurjchem-376	89	19	=	=	SYM
eurjchem-376	89	20	n	n	NUM
eurjchem-376	89	21	)	)	PUNCT
eurjchem-376	89	22	,	,	PUNCT
eurjchem-376	89	23	1605	1605	NUM
eurjchem-376	89	24	(c	(c	PROPN
eurjchem-376	89	25	=	=	SYM
eurjchem-376	89	26	c	c	NOUN
eurjchem-376	89	27	)	)	PUNCT
eurjchem-376	89	28	.	.	PUNCT
eurjchem-376	90	1	1h	1h	NUM
eurjchem-376	90	2	nmr	nmr	NOUN
eurjchem-376	90	3	(	(	PUNCT
eurjchem-376	90	4	200	200	NUM
eurjchem-376	90	5	mhz	mhz	NOUN
eurjchem-376	90	6	,	,	PUNCT
eurjchem-376	90	7	dmso‐d6	dmso‐d6	NUM
eurjchem-376	90	8	):	):	PUNCT
eurjchem-376	90	9	6.97‐7.94	6.97‐7.94	NUM
eurjchem-376	90	10	(	(	PUNCT
eurjchem-376	90	11	m	m	PROPN
eurjchem-376	90	12	,	,	PUNCT
eurjchem-376	90	13	14h	14h	NUM
eurjchem-376	90	14	,	,	PUNCT
eurjchem-376	90	15	arh	arh	PROPN
eurjchem-376	90	16	)	)	PUNCT
eurjchem-376	90	17	,	,	PUNCT
eurjchem-376	90	18	8.32	8.32	NUM
eurjchem-376	90	19	(	(	PUNCT
eurjchem-376	90	20	s	s	PROPN
eurjchem-376	90	21	,	,	PUNCT
eurjchem-376	90	22	1h	1h	NUM
eurjchem-376	90	23	,	,	PUNCT
eurjchem-376	90	24	nh	nh	PROPN
eurjchem-376	90	25	,	,	PUNCT
eurjchem-376	90	26	exchangeable	exchangeable	ADJ
eurjchem-376	90	27	)	)	PUNCT
eurjchem-376	90	28	,	,	PUNCT
eurjchem-376	90	29	9.22	9.22	NUM
eurjchem-376	90	30	(	(	PUNCT
eurjchem-376	90	31	s	s	PROPN
eurjchem-376	90	32	,	,	PUNCT
eurjchem-376	90	33	1h	1h	NUM
eurjchem-376	90	34	,	,	PUNCT
eurjchem-376	90	35	oh	oh	INTJ
eurjchem-376	90	36	,	,	PUNCT
eurjchem-376	90	37	exchangeable	exchangeable	ADJ
eurjchem-376	90	38	)	)	PUNCT
eurjchem-376	90	39	.	.	PUNCT
eurjchem-376	91	1	ms	ms	NOUN
eurjchem-376	91	2	(	(	PUNCT
eurjchem-376	91	3	m	m	PROPN
eurjchem-376	91	4	/	/	SYM
eurjchem-376	91	5	z	z	NOUN
eurjchem-376	91	6	):	):	PUNCT
eurjchem-376	91	7	464	464	NUM
eurjchem-376	91	8	(	(	PUNCT
eurjchem-376	91	9	m+	m+	NUM
eurjchem-376	91	10	)	)	PUNCT
eurjchem-376	91	11	.	.	PUNCT
eurjchem-376	92	1	anal	anal	PROPN
eurjchem-376	92	2	.	.	PUNCT
eurjchem-376	92	3	calcd	calcd	NOUN
eurjchem-376	92	4	.	.	PUNCT
eurjchem-376	93	1	for	for	ADP
eurjchem-376	93	2	c25h16n6o2s	c25h16n6o2s	NOUN
eurjchem-376	93	3	:	:	PUNCT
eurjchem-376	93	4	c	c	X
eurjchem-376	93	5	,	,	PUNCT
eurjchem-376	93	6	64.64	64.64	NUM
eurjchem-376	93	7	;	;	PUNCT
eurjchem-376	93	8	h	h	X
eurjchem-376	93	9	,	,	PUNCT
eurjchem-376	93	10	3.47	3.47	NUM
eurjchem-376	93	11	;	;	PUNCT
eurjchem-376	93	12	n	n	CCONJ
eurjchem-376	93	13	,	,	PUNCT
eurjchem-376	93	14	18.09	18.09	NUM
eurjchem-376	93	15	.	.	PUNCT
eurjchem-376	93	16	found	find	VERB
eurjchem-376	93	17	:	:	PUNCT
eurjchem-376	94	1	c	c	X
eurjchem-376	94	2	,	,	PUNCT
eurjchem-376	94	3	64.42	64.42	NUM
eurjchem-376	94	4	;	;	PUNCT
eurjchem-376	94	5	h	h	NOUN
eurjchem-376	94	6	,	,	PUNCT
eurjchem-376	94	7	3.3	3.3	NUM
eurjchem-376	94	8	;	;	PUNCT
eurjchem-376	94	9	n	n	CCONJ
eurjchem-376	94	10	,	,	PUNCT
eurjchem-376	94	11	17.89	17.89	NUM
eurjchem-376	94	12	%	%	NOUN
eurjchem-376	94	13	.	.	PUNCT
eurjchem-376	95	1	2.1.7	2.1.7	X
eurjchem-376	95	2	.	.	PUNCT
eurjchem-376	96	1	5‐acetyl‐n‐(6‐dibenzothiophen‐2‐yl	5‐acetyl‐n‐(6‐dibenzothiophen‐2‐yl	NUM
eurjchem-376	96	2	–	–	PUNCT
eurjchem-376	96	3	pyridazin‐3‐yl)‐4‐	pyridazin‐3‐yl)‐4‐	NOUN
eurjchem-376	96	4	hydroxy‐2‐(phenylamino	hydroxy‐2‐(phenylamino	NOUN
eurjchem-376	96	5	)	)	PUNCT
eurjchem-376	96	6	thiophene‐3‐carboxamide	thiophene‐3‐carboxamide	X
eurjchem-376	96	7	(	(	PUNCT
eurjchem-376	96	8	10	10	NUM
eurjchem-376	96	9	)	)	PUNCT
eurjchem-376	96	10	phenyl	phenyl	NOUN
eurjchem-376	96	11	isothiocyanate	isothiocyanate	NOUN
eurjchem-376	96	12	(	(	PUNCT
eurjchem-376	96	13	0.01	0.01	NUM
eurjchem-376	96	14	mol	mol	NOUN
eurjchem-376	96	15	)	)	PUNCT
eurjchem-376	96	16	was	be	AUX
eurjchem-376	96	17	added	add	VERB
eurjchem-376	96	18	to	to	ADP
eurjchem-376	96	19	a	a	DET
eurjchem-376	96	20	solution	solution	NOUN
eurjchem-376	96	21	of	of	ADP
eurjchem-376	96	22	2	2	NUM
eurjchem-376	96	23	(	(	PUNCT
eurjchem-376	96	24	0.01	0.01	NUM
eurjchem-376	96	25	mol	mol	NOUN
eurjchem-376	96	26	)	)	PUNCT
eurjchem-376	96	27	in	in	ADP
eurjchem-376	96	28	dimethylformamide	dimethylformamide	NOUN
eurjchem-376	96	29	(	(	PUNCT
eurjchem-376	96	30	30	30	NUM
eurjchem-376	96	31	ml	ml	NOUN
eurjchem-376	96	32	)	)	PUNCT
eurjchem-376	96	33	containing	contain	VERB
eurjchem-376	96	34	potassium	potassium	NOUN
eurjchem-376	96	35	hydroxide	hydroxide	NOUN
eurjchem-376	96	36	(	(	PUNCT
eurjchem-376	96	37	0.01	0.01	NUM
eurjchem-376	96	38	mol	mol	NOUN
eurjchem-376	96	39	)	)	PUNCT
eurjchem-376	96	40	.	.	PUNCT
eurjchem-376	97	1	the	the	DET
eurjchem-376	97	2	reaction	reaction	NOUN
eurjchem-376	97	3	mixture	mixture	NOUN
eurjchem-376	97	4	was	be	AUX
eurjchem-376	97	5	stirred	stir	VERB
eurjchem-376	97	6	at	at	ADP
eurjchem-376	97	7	room	room	NOUN
eurjchem-376	97	8	temperature	temperature	NOUN
eurjchem-376	97	9	overnight	overnight	ADV
eurjchem-376	97	10	.	.	PUNCT
eurjchem-376	98	1	then	then	ADV
eurjchem-376	98	2	chloroacetone	chloroacetone	NOUN
eurjchem-376	98	3	(	(	PUNCT
eurjchem-376	98	4	0.01	0.01	NUM
eurjchem-376	98	5	mol	mol	NOUN
eurjchem-376	98	6	)	)	PUNCT
eurjchem-376	98	7	was	be	AUX
eurjchem-376	98	8	added	add	VERB
eurjchem-376	98	9	to	to	ADP
eurjchem-376	98	10	the	the	DET
eurjchem-376	98	11	reaction	reaction	NOUN
eurjchem-376	98	12	mixture	mixture	NOUN
eurjchem-376	98	13	and	and	CCONJ
eurjchem-376	98	14	all	all	PRON
eurjchem-376	98	15	was	be	AUX
eurjchem-376	98	16	stirred	stir	VERB
eurjchem-376	98	17	at	at	ADP
eurjchem-376	98	18	room	room	NOUN
eurjchem-376	98	19	temperature	temperature	NOUN
eurjchem-376	98	20	overnight	overnight	ADV
eurjchem-376	98	21	.	.	PUNCT
eurjchem-376	99	1	the	the	DET
eurjchem-376	99	2	mixture	mixture	NOUN
eurjchem-376	99	3	was	be	AUX
eurjchem-376	99	4	poured	pour	VERB
eurjchem-376	99	5	into	into	ADP
eurjchem-376	99	6	crushed	crushed	ADJ
eurjchem-376	99	7	ice	ice	NOUN
eurjchem-376	99	8	and	and	CCONJ
eurjchem-376	99	9	hydrochloric	hydrochloric	ADJ
eurjchem-376	99	10	acid	acid	NOUN
eurjchem-376	99	11	.	.	PUNCT
eurjchem-376	100	1	the	the	DET
eurjchem-376	100	2	precipitated	precipitate	VERB
eurjchem-376	100	3	solid	solid	ADJ
eurjchem-376	100	4	was	be	AUX
eurjchem-376	100	5	collected	collect	VERB
eurjchem-376	100	6	by	by	ADP
eurjchem-376	100	7	filtration	filtration	NOUN
eurjchem-376	100	8	,	,	PUNCT
eurjchem-376	100	9	washed	wash	VERB
eurjchem-376	100	10	and	and	CCONJ
eurjchem-376	100	11	dried	dry	VERB
eurjchem-376	100	12	:	:	PUNCT
eurjchem-376	100	13	yellow	yellow	ADJ
eurjchem-376	100	14	,	,	PUNCT
eurjchem-376	100	15	yield	yield	NOUN
eurjchem-376	100	16	:	:	PUNCT
eurjchem-376	100	17	62	62	NUM
eurjchem-376	100	18	%	%	NOUN
eurjchem-376	100	19	(	(	PUNCT
eurjchem-376	100	20	ethanol	ethanol	NOUN
eurjchem-376	100	21	)	)	PUNCT
eurjchem-376	100	22	(	(	PUNCT
eurjchem-376	100	23	scheme	scheme	NOUN
eurjchem-376	100	24	3	3	NUM
eurjchem-376	100	25	)	)	PUNCT
eurjchem-376	100	26	.	.	PUNCT
eurjchem-376	101	1	m.p	m.p	PROPN
eurjchem-376	101	2	.	.	PROPN
eurjchem-376	101	3	:	:	PUNCT
eurjchem-376	102	1	175‐177	175‐177	NUM
eurjchem-376	102	2	c	c	ADJ
eurjchem-376	102	3	.	.	PUNCT
eurjchem-376	103	1	ir	ir	PROPN
eurjchem-376	103	2	(	(	PUNCT
eurjchem-376	103	3	kbr	kbr	PROPN
eurjchem-376	103	4	,	,	PUNCT
eurjchem-376	103	5	cm‐1	cm‐1	PROPN
eurjchem-376	103	6	):	):	PUNCT
eurjchem-376	103	7	3420‐3270	3420‐3270	NUM
eurjchem-376	103	8	(oh	(oh	NOUN
eurjchem-376	103	9	,	,	PUNCT
eurjchem-376	103	10	nh	nh	PROPN
eurjchem-376	103	11	)	)	PUNCT
eurjchem-376	103	12	,	,	PUNCT
eurjchem-376	103	13	1690	1690	NUM
eurjchem-376	103	14	,	,	PUNCT
eurjchem-376	103	15	1675	1675	NUM
eurjchem-376	103	16	(co	(co	NOUN
eurjchem-376	103	17	)	)	PUNCT
eurjchem-376	103	18	,	,	PUNCT
eurjchem-376	103	19	1630	1630	NUM
eurjchem-376	103	20	(c	(c	PROPN
eurjchem-376	103	21	=	=	SYM
eurjchem-376	103	22	c	c	NOUN
eurjchem-376	103	23	)	)	PUNCT
eurjchem-376	103	24	.	.	PUNCT
eurjchem-376	104	1	1h	1h	NUM
eurjchem-376	104	2	nmr	nmr	NOUN
eurjchem-376	104	3	(	(	PUNCT
eurjchem-376	104	4	200	200	NUM
eurjchem-376	104	5	mhz	mhz	NOUN
eurjchem-376	104	6	,	,	PUNCT
eurjchem-376	104	7	cdcl3	cdcl3	NOUN
eurjchem-376	104	8	):	):	PUNCT
eurjchem-376	104	9	2.30	2.30	NUM
eurjchem-376	104	10	(	(	PUNCT
eurjchem-376	104	11	s	s	PROPN
eurjchem-376	104	12	,	,	PUNCT
eurjchem-376	104	13	3h	3h	NUM
eurjchem-376	104	14	,	,	PUNCT
eurjchem-376	104	15	ch3	ch3	PROPN
eurjchem-376	104	16	)	)	PUNCT
eurjchem-376	104	17	,	,	PUNCT
eurjchem-376	104	18	7.06‐7.94	7.06‐7.94	NUM
eurjchem-376	104	19	(	(	PUNCT
eurjchem-376	104	20	m	m	PROPN
eurjchem-376	104	21	,	,	PUNCT
eurjchem-376	104	22	14h	14h	NUM
eurjchem-376	104	23	,	,	PUNCT
eurjchem-376	104	24	ar‐h	ar‐h	NOUN
eurjchem-376	104	25	)	)	PUNCT
eurjchem-376	104	26	,	,	PUNCT
eurjchem-376	104	27	8.41	8.41	NUM
eurjchem-376	104	28	,	,	PUNCT
eurjchem-376	104	29	8.83	8.83	NUM
eurjchem-376	104	30	(	(	PUNCT
eurjchem-376	104	31	2s	2s	NUM
eurjchem-376	104	32	,	,	PUNCT
eurjchem-376	104	33	2h	2h	NUM
eurjchem-376	104	34	,	,	PUNCT
eurjchem-376	104	35	2nh	2nh	NOUN
eurjchem-376	104	36	,	,	PUNCT
eurjchem-376	104	37	exchangeable	exchangeable	ADJ
eurjchem-376	104	38	)	)	PUNCT
eurjchem-376	104	39	,	,	PUNCT
eurjchem-376	104	40	10.26	10.26	NUM
eurjchem-376	104	41	(	(	PUNCT
eurjchem-376	104	42	s	s	PROPN
eurjchem-376	104	43	,	,	PUNCT
eurjchem-376	104	44	1h	1h	NUM
eurjchem-376	104	45	,	,	PUNCT
eurjchem-376	104	46	oh	oh	INTJ
eurjchem-376	104	47	,	,	PUNCT
eurjchem-376	104	48	exchangeable	exchangeable	ADJ
eurjchem-376	104	49	)	)	PUNCT
eurjchem-376	104	50	.	.	PUNCT
eurjchem-376	105	1	13c	13c	NOUN
eurjchem-376	105	2	nmr	nmr	NOUN
eurjchem-376	105	3	(	(	PUNCT
eurjchem-376	105	4	50	50	NUM
eurjchem-376	105	5	mhz	mhz	NOUN
eurjchem-376	105	6	,	,	PUNCT
eurjchem-376	105	7	cdcl3	cdcl3	NOUN
eurjchem-376	105	8	):	):	PUNCT
eurjchem-376	105	9	20.4	20.4	NUM
eurjchem-376	105	10	(	(	PUNCT
eurjchem-376	105	11	ch3	ch3	PROPN
eurjchem-376	105	12	)	)	PUNCT
eurjchem-376	105	13	,	,	PUNCT
eurjchem-376	105	14	114.5	114.5	NUM
eurjchem-376	105	15	,	,	PUNCT
eurjchem-376	105	16	118.2	118.2	NUM
eurjchem-376	105	17	,	,	PUNCT
eurjchem-376	105	18	127.1	127.1	NUM
eurjchem-376	105	19	,	,	PUNCT
eurjchem-376	105	20	142.1	142.1	NUM
eurjchem-376	105	21	(	(	PUNCT
eurjchem-376	105	22	phenyl	phenyl	NOUN
eurjchem-376	105	23	carbons	carbon	NOUN
eurjchem-376	105	24	)	)	PUNCT
eurjchem-376	105	25	,	,	PUNCT
eurjchem-376	105	26	125.3	125.3	NUM
eurjchem-376	105	27	,	,	PUNCT
eurjchem-376	105	28	135.2	135.2	NUM
eurjchem-376	105	29	,	,	PUNCT
eurjchem-376	105	30	148.5	148.5	NUM
eurjchem-376	105	31	,	,	PUNCT
eurjchem-376	105	32	151.1	151.1	NUM
eurjchem-376	105	33	(	(	PUNCT
eurjchem-376	105	34	thiophene	thiophene	NOUN
eurjchem-376	105	35	carbons	carbon	NOUN
eurjchem-376	105	36	)	)	PUNCT
eurjchem-376	105	37	,	,	PUNCT
eurjchem-376	105	38	118.6	118.6	NUM
eurjchem-376	105	39	,	,	PUNCT
eurjchem-376	105	40	121.1	121.1	NUM
eurjchem-376	105	41	,	,	PUNCT
eurjchem-376	105	42	121.5	121.5	NUM
eurjchem-376	105	43	,	,	PUNCT
eurjchem-376	105	44	122.2	122.2	NUM
eurjchem-376	105	45	,	,	PUNCT
eurjchem-376	105	46	122.8	122.8	NUM
eurjchem-376	105	47	,	,	PUNCT
eurjchem-376	105	48	123.2	123.2	NUM
eurjchem-376	105	49	,	,	PUNCT
eurjchem-376	105	50	124.1	124.1	NUM
eurjchem-376	105	51	,	,	PUNCT
eurjchem-376	105	52	124.8	124.8	NUM
eurjchem-376	105	53	,	,	PUNCT
eurjchem-376	105	54	125.4	125.4	NUM
eurjchem-376	105	55	,	,	PUNCT
eurjchem-376	105	56	127.3	127.3	NUM
eurjchem-376	105	57	,	,	PUNCT
eurjchem-376	105	58	128.5	128.5	NUM
eurjchem-376	105	59	,	,	PUNCT
eurjchem-376	105	60	131.2	131.2	NUM
eurjchem-376	105	61	,	,	PUNCT
eurjchem-376	105	62	136.6	136.6	NUM
eurjchem-376	105	63	,	,	PUNCT
eurjchem-376	105	64	138.2	138.2	NUM
eurjchem-376	105	65	,	,	PUNCT
eurjchem-376	105	66	146.3	146.3	NUM
eurjchem-376	105	67	,	,	PUNCT
eurjchem-376	105	68	150.4	150.4	NUM
eurjchem-376	105	69	(	(	PUNCT
eurjchem-376	105	70	dibenzothiophene	dibenzothiophene	ADJ
eurjchem-376	105	71	and	and	CCONJ
eurjchem-376	105	72	pyridazine	pyridazine	NOUN
eurjchem-376	105	73	carbons	carbon	NOUN
eurjchem-376	105	74	)	)	PUNCT
eurjchem-376	105	75	,	,	PUNCT
eurjchem-376	105	76	178.5	178.5	NUM
eurjchem-376	105	77	,	,	PUNCT
eurjchem-376	105	78	182.2	182.2	NUM
eurjchem-376	105	79	(	(	PUNCT
eurjchem-376	105	80	2co	2co	NOUN
eurjchem-376	105	81	)	)	PUNCT
eurjchem-376	105	82	.	.	PUNCT
eurjchem-376	106	1	ms	ms	NOUN
eurjchem-376	106	2	(	(	PUNCT
eurjchem-376	106	3	m	m	PROPN
eurjchem-376	106	4	/	/	SYM
eurjchem-376	106	5	z	z	NOUN
eurjchem-376	106	6	):	):	PUNCT
eurjchem-376	106	7	536	536	NUM
eurjchem-376	106	8	(	(	PUNCT
eurjchem-376	106	9	m+	m+	NUM
eurjchem-376	106	10	)	)	PUNCT
eurjchem-376	106	11	.	.	PUNCT
eurjchem-376	107	1	anal	anal	PROPN
eurjchem-376	107	2	.	.	PUNCT
eurjchem-376	107	3	calcd	calcd	NOUN
eurjchem-376	107	4	.	.	PUNCT
eurjchem-376	108	1	for	for	ADP
eurjchem-376	108	2	c29h20n4o3s2	c29h20n4o3s2	NOUN
eurjchem-376	108	3	:	:	PUNCT
eurjchem-376	108	4	c	c	X
eurjchem-376	108	5	,	,	PUNCT
eurjchem-376	108	6	64.91	64.91	NUM
eurjchem-376	108	7	;	;	PUNCT
eurjchem-376	108	8	h	h	NOUN
eurjchem-376	108	9	,	,	PUNCT
eurjchem-376	108	10	3.76	3.76	NUM
eurjchem-376	108	11	;	;	PUNCT
eurjchem-376	108	12	n	n	CCONJ
eurjchem-376	108	13	,	,	PUNCT
eurjchem-376	108	14	10.44	10.44	NUM
eurjchem-376	108	15	.	.	PUNCT
eurjchem-376	108	16	found	find	VERB
eurjchem-376	108	17	:	:	PUNCT
eurjchem-376	109	1	c	c	X
eurjchem-376	109	2	,	,	PUNCT
eurjchem-376	109	3	64.80	64.80	NUM
eurjchem-376	109	4	;	;	PUNCT
eurjchem-376	109	5	h	h	NOUN
eurjchem-376	109	6	,	,	PUNCT
eurjchem-376	109	7	3.64	3.64	NUM
eurjchem-376	109	8	;	;	PUNCT
eurjchem-376	109	9	n	n	CCONJ
eurjchem-376	109	10	,	,	PUNCT
eurjchem-376	109	11	10.32	10.32	NUM
eurjchem-376	109	12	%	%	NOUN
eurjchem-376	109	13	.	.	PUNCT
eurjchem-376	110	1	behalo	behalo	NOUN
eurjchem-376	110	2	and	and	CCONJ
eurjchem-376	110	3	aly	aly	PROPN
eurjchem-376	110	4	/	/	SYM
eurjchem-376	110	5	european	european	PROPN
eurjchem-376	110	6	journal	journal	PROPN
eurjchem-376	110	7	of	of	ADP
eurjchem-376	110	8	chemistry	chemistry	NOUN
eurjchem-376	110	9	2	2	NUM
eurjchem-376	110	10	(	(	PUNCT
eurjchem-376	110	11	3	3	NUM
eurjchem-376	110	12	)	)	PUNCT
eurjchem-376	110	13	(	(	PUNCT
eurjchem-376	110	14	2011	2011	NUM
eurjchem-376	110	15	)	)	PUNCT
eurjchem-376	110	16	295‐299	295‐299	NOUN
eurjchem-376	111	1	297	297	NUM
eurjchem-376	111	2	scheme	scheme	NOUN
eurjchem-376	111	3	3	3	NUM
eurjchem-376	111	4	2.1.8	2.1.8	NUM
eurjchem-376	111	5	.	.	PUNCT
eurjchem-376	111	6	general	general	ADJ
eurjchem-376	111	7	procedure	procedure	NOUN
eurjchem-376	111	8	for	for	ADP
eurjchem-376	111	9	the	the	DET
eurjchem-376	111	10	synthesis	synthesis	NOUN
eurjchem-376	111	11	of	of	ADP
eurjchem-376	111	12	11a	11a	NOUN
eurjchem-376	111	13	,	,	PUNCT
eurjchem-376	111	14	b	b	NOUN
eurjchem-376	111	15	a	a	DET
eurjchem-376	111	16	mixture	mixture	NOUN
eurjchem-376	111	17	of	of	ADP
eurjchem-376	111	18	ester	ester	NOUN
eurjchem-376	111	19	2	2	NUM
eurjchem-376	111	20	(	(	PUNCT
eurjchem-376	111	21	0.01	0.01	NUM
eurjchem-376	111	22	mol	mol	NOUN
eurjchem-376	111	23	)	)	PUNCT
eurjchem-376	111	24	and	and	CCONJ
eurjchem-376	111	25	urea	urea	NOUN
eurjchem-376	111	26	or	or	CCONJ
eurjchem-376	111	27	thiourea	thiourea	NOUN
eurjchem-376	111	28	(	(	PUNCT
eurjchem-376	111	29	0.01	0.01	NUM
eurjchem-376	111	30	mol	mol	NOUN
eurjchem-376	111	31	)	)	PUNCT
eurjchem-376	111	32	was	be	AUX
eurjchem-376	111	33	heated	heat	VERB
eurjchem-376	111	34	in	in	ADP
eurjchem-376	111	35	ethanol	ethanol	NOUN
eurjchem-376	111	36	(	(	PUNCT
eurjchem-376	111	37	30	30	NUM
eurjchem-376	111	38	ml	ml	NOUN
eurjchem-376	111	39	)	)	PUNCT
eurjchem-376	111	40	containing	contain	VERB
eurjchem-376	111	41	sodium	sodium	NOUN
eurjchem-376	111	42	ethoxide	ethoxide	ADV
eurjchem-376	111	43	under	under	ADP
eurjchem-376	111	44	reflux	reflux	NOUN
eurjchem-376	111	45	for	for	ADP
eurjchem-376	111	46	6	6	NUM
eurjchem-376	111	47	hours	hour	NOUN
eurjchem-376	111	48	then	then	ADV
eurjchem-376	111	49	left	leave	VERB
eurjchem-376	111	50	to	to	PART
eurjchem-376	111	51	cool	cool	ADJ
eurjchem-376	111	52	.	.	PUNCT
eurjchem-376	112	1	the	the	DET
eurjchem-376	112	2	reaction	reaction	NOUN
eurjchem-376	112	3	mixture	mixture	NOUN
eurjchem-376	112	4	was	be	AUX
eurjchem-376	112	5	poured	pour	VERB
eurjchem-376	112	6	into	into	ADP
eurjchem-376	112	7	cold	cold	ADJ
eurjchem-376	112	8	water	water	NOUN
eurjchem-376	112	9	and	and	CCONJ
eurjchem-376	112	10	the	the	DET
eurjchem-376	112	11	formed	form	VERB
eurjchem-376	112	12	solid	solid	ADJ
eurjchem-376	112	13	product	product	NOUN
eurjchem-376	112	14	was	be	AUX
eurjchem-376	112	15	collected	collect	VERB
eurjchem-376	112	16	by	by	ADP
eurjchem-376	112	17	filtration	filtration	NOUN
eurjchem-376	112	18	,	,	PUNCT
eurjchem-376	112	19	washed	wash	VERB
eurjchem-376	112	20	,	,	PUNCT
eurjchem-376	112	21	dried	dry	VERB
eurjchem-376	112	22	and	and	CCONJ
eurjchem-376	112	23	recrystallized	recrystallize	VERB
eurjchem-376	112	24	(	(	PUNCT
eurjchem-376	112	25	scheme	scheme	NOUN
eurjchem-376	112	26	4	4	NUM
eurjchem-376	112	27	)	)	PUNCT
eurjchem-376	112	28	.	.	PUNCT
eurjchem-376	113	1	6‐(6‐dibenzothiophen‐2‐yl	6‐(6‐dibenzothiophen‐2‐yl	PROPN
eurjchem-376	113	2	–	–	PUNCT
eurjchem-376	113	3	pyridazin‐3‐ylamino)pyrimidine‐	pyridazin‐3‐ylamino)pyrimidine‐	PROPN
eurjchem-376	113	4	2,4(3h,5h)‐dione	2,4(3h,5h)‐dione	NUM
eurjchem-376	113	5	(	(	PUNCT
eurjchem-376	113	6	11a	11a	NUM
eurjchem-376	113	7	):	):	PUNCT
eurjchem-376	113	8	yellow	yellow	ADJ
eurjchem-376	113	9	,	,	PUNCT
eurjchem-376	113	10	yield	yield	NOUN
eurjchem-376	113	11	:	:	PUNCT
eurjchem-376	113	12	77	77	NUM
eurjchem-376	113	13	%	%	NOUN
eurjchem-376	113	14	(	(	PUNCT
eurjchem-376	113	15	butanol	butanol	NOUN
eurjchem-376	113	16	)	)	PUNCT
eurjchem-376	113	17	.	.	PUNCT
eurjchem-376	114	1	m.p	m.p	PROPN
eurjchem-376	114	2	.	.	PROPN
eurjchem-376	114	3	:	:	PUNCT
eurjchem-376	115	1	210‐212	210‐212	NUM
eurjchem-376	115	2	c	c	ADJ
eurjchem-376	115	3	.	.	PUNCT
eurjchem-376	116	1	ir	ir	PROPN
eurjchem-376	116	2	(	(	PUNCT
eurjchem-376	116	3	kbr	kbr	PROPN
eurjchem-376	116	4	,	,	PUNCT
eurjchem-376	116	5	cm‐1	cm‐1	PROPN
eurjchem-376	116	6	):	):	PUNCT
eurjchem-376	116	7	3440‐3250	3440‐3250	NUM
eurjchem-376	116	8	(oh	(oh	NOUN
eurjchem-376	116	9	,	,	PUNCT
eurjchem-376	116	10	nh	nh	PROPN
eurjchem-376	116	11	)	)	PUNCT
eurjchem-376	116	12	,	,	PUNCT
eurjchem-376	116	13	1682	1682	NUM
eurjchem-376	116	14	,	,	PUNCT
eurjchem-376	116	15	1665	1665	NUM
eurjchem-376	116	16	(co	(co	NOUN
eurjchem-376	116	17	)	)	PUNCT
eurjchem-376	116	18	,	,	PUNCT
eurjchem-376	116	19	1610	1610	NUM
eurjchem-376	116	20	(c	(c	PROPN
eurjchem-376	116	21	=	=	SYM
eurjchem-376	116	22	n	n	NUM
eurjchem-376	116	23	)	)	PUNCT
eurjchem-376	116	24	.	.	PUNCT
eurjchem-376	117	1	1h	1h	NUM
eurjchem-376	117	2	nmr	nmr	NOUN
eurjchem-376	117	3	(	(	PUNCT
eurjchem-376	117	4	200	200	NUM
eurjchem-376	117	5	mhz	mhz	NOUN
eurjchem-376	117	6	,	,	PUNCT
eurjchem-376	117	7	cdcl3	cdcl3	NOUN
eurjchem-376	117	8	):	):	PUNCT
eurjchem-376	117	9	3.21	3.21	NUM
eurjchem-376	117	10	(	(	PUNCT
eurjchem-376	117	11	s	s	PROPN
eurjchem-376	117	12	,	,	PUNCT
eurjchem-376	117	13	2h	2h	NUM
eurjchem-376	117	14	,	,	PUNCT
eurjchem-376	117	15	ch2	ch2	PROPN
eurjchem-376	117	16	)	)	PUNCT
eurjchem-376	117	17	,	,	PUNCT
eurjchem-376	117	18	6.84‐8.01	6.84‐8.01	NUM
eurjchem-376	117	19	(	(	PUNCT
eurjchem-376	117	20	m	m	PROPN
eurjchem-376	117	21	,	,	PUNCT
eurjchem-376	117	22	9h	9h	NUM
eurjchem-376	117	23	,	,	PUNCT
eurjchem-376	117	24	ar‐h	ar‐h	NOUN
eurjchem-376	117	25	)	)	PUNCT
eurjchem-376	117	26	,	,	PUNCT
eurjchem-376	117	27	8.33	8.33	NUM
eurjchem-376	117	28	,	,	PUNCT
eurjchem-376	117	29	9.81	9.81	NUM
eurjchem-376	117	30	(	(	PUNCT
eurjchem-376	117	31	2s	2s	NUM
eurjchem-376	117	32	,	,	PUNCT
eurjchem-376	117	33	2h	2h	NUM
eurjchem-376	117	34	,	,	PUNCT
eurjchem-376	117	35	2nh	2nh	NOUN
eurjchem-376	117	36	,	,	PUNCT
eurjchem-376	117	37	exchangeable	exchangeable	ADJ
eurjchem-376	117	38	)	)	PUNCT
eurjchem-376	117	39	.	.	PUNCT
eurjchem-376	118	1	anal	anal	PROPN
eurjchem-376	118	2	.	.	PUNCT
eurjchem-376	118	3	calcd	calcd	NOUN
eurjchem-376	118	4	.	.	PUNCT
eurjchem-376	119	1	for	for	SCONJ
eurjchem-376	119	2	c20h13n5o2s	c20h13n5o2s	PROPN
eurjchem-376	119	3	:	:	PUNCT
eurjchem-376	119	4	c	c	X
eurjchem-376	119	5	,	,	PUNCT
eurjchem-376	119	6	62.00	62.00	NUM
eurjchem-376	119	7	;	;	PUNCT
eurjchem-376	119	8	h	h	NOUN
eurjchem-376	119	9	,	,	PUNCT
eurjchem-376	119	10	3.38	3.38	NUM
eurjchem-376	119	11	;	;	PUNCT
eurjchem-376	119	12	n	n	CCONJ
eurjchem-376	119	13	,	,	PUNCT
eurjchem-376	119	14	18.08	18.08	NUM
eurjchem-376	119	15	.	.	PUNCT
eurjchem-376	119	16	found	find	VERB
eurjchem-376	119	17	:	:	PUNCT
eurjchem-376	120	1	c	c	X
eurjchem-376	120	2	,	,	PUNCT
eurjchem-376	120	3	61.82	61.82	NUM
eurjchem-376	120	4	;	;	PUNCT
eurjchem-376	120	5	h	h	X
eurjchem-376	120	6	,	,	PUNCT
eurjchem-376	120	7	3.16	3.16	NUM
eurjchem-376	120	8	;	;	PUNCT
eurjchem-376	120	9	n	n	CCONJ
eurjchem-376	120	10	,	,	PUNCT
eurjchem-376	120	11	17.88	17.88	NUM
eurjchem-376	120	12	%	%	NOUN
eurjchem-376	120	13	.	.	PUNCT
eurjchem-376	121	1	6‐(6‐dibenzothiophen‐2‐yl	6‐(6‐dibenzothiophen‐2‐yl	PROPN
eurjchem-376	121	2	–	–	PUNCT
eurjchem-376	121	3	pyridazin‐3‐ylamino)‐2‐thioxo‐	pyridazin‐3‐ylamino)‐2‐thioxo‐	PROPN
eurjchem-376	121	4	2,3‐dihydropyrimidine‐4(5h)‐one	2,3‐dihydropyrimidine‐4(5h)‐one	NUM
eurjchem-376	121	5	(	(	PUNCT
eurjchem-376	121	6	11b	11b	NOUN
eurjchem-376	121	7	):	):	PUNCT
eurjchem-376	121	8	yellow	yellow	ADJ
eurjchem-376	121	9	,	,	PUNCT
eurjchem-376	121	10	yield	yield	NOUN
eurjchem-376	121	11	:	:	PUNCT
eurjchem-376	121	12	71	71	NUM
eurjchem-376	121	13	%	%	NOUN
eurjchem-376	121	14	(	(	PUNCT
eurjchem-376	121	15	butanol	butanol	NOUN
eurjchem-376	121	16	)	)	PUNCT
eurjchem-376	121	17	.	.	PUNCT
eurjchem-376	122	1	m.p	m.p	PROPN
eurjchem-376	122	2	.	.	PROPN
eurjchem-376	122	3	:	:	PUNCT
eurjchem-376	123	1	195‐197	195‐197	NUM
eurjchem-376	123	2	c	c	ADJ
eurjchem-376	123	3	.	.	PUNCT
eurjchem-376	124	1	ir	ir	PROPN
eurjchem-376	124	2	(	(	PUNCT
eurjchem-376	124	3	kbr	kbr	PROPN
eurjchem-376	124	4	,	,	PUNCT
eurjchem-376	124	5	cm‐1	cm‐1	PROPN
eurjchem-376	124	6	):	):	PUNCT
eurjchem-376	124	7	3420‐3180	3420‐3180	PROPN
eurjchem-376	124	8	(oh	(oh	NOUN
eurjchem-376	124	9	,	,	PUNCT
eurjchem-376	124	10	nh	nh	PROPN
eurjchem-376	124	11	)	)	PUNCT
eurjchem-376	124	12	,	,	PUNCT
eurjchem-376	124	13	1680	1680	NUM
eurjchem-376	124	14	(co	(co	NOUN
eurjchem-376	124	15	)	)	PUNCT
eurjchem-376	124	16	,	,	PUNCT
eurjchem-376	124	17	1625	1625	NUM
eurjchem-376	124	18	(c	(c	PROPN
eurjchem-376	124	19	=	=	SYM
eurjchem-376	124	20	n	n	NUM
eurjchem-376	124	21	)	)	PUNCT
eurjchem-376	124	22	.	.	PUNCT
eurjchem-376	125	1	1h	1h	NUM
eurjchem-376	125	2	nmr	nmr	NOUN
eurjchem-376	125	3	(	(	PUNCT
eurjchem-376	125	4	200	200	NUM
eurjchem-376	125	5	mhz	mhz	NOUN
eurjchem-376	125	6	,	,	PUNCT
eurjchem-376	125	7	cdcl3	cdcl3	NOUN
eurjchem-376	125	8	):	):	PUNCT
eurjchem-376	125	9	2.92	2.92	NUM
eurjchem-376	125	10	(	(	PUNCT
eurjchem-376	125	11	s	s	PROPN
eurjchem-376	125	12	,	,	PUNCT
eurjchem-376	125	13	2h	2h	NUM
eurjchem-376	125	14	,	,	PUNCT
eurjchem-376	125	15	ch2	ch2	PROPN
eurjchem-376	125	16	)	)	PUNCT
eurjchem-376	125	17	,	,	PUNCT
eurjchem-376	125	18	7.16‐7.94	7.16‐7.94	NUM
eurjchem-376	125	19	(	(	PUNCT
eurjchem-376	125	20	m	m	PROPN
eurjchem-376	125	21	,	,	PUNCT
eurjchem-376	125	22	9h	9h	NUM
eurjchem-376	125	23	,	,	PUNCT
eurjchem-376	125	24	ar‐h	ar‐h	NOUN
eurjchem-376	125	25	)	)	PUNCT
eurjchem-376	125	26	,	,	PUNCT
eurjchem-376	125	27	8.52	8.52	NUM
eurjchem-376	125	28	,	,	PUNCT
eurjchem-376	125	29	9.80	9.80	NUM
eurjchem-376	125	30	(	(	PUNCT
eurjchem-376	125	31	2s	2s	NUM
eurjchem-376	125	32	,	,	PUNCT
eurjchem-376	125	33	2h	2h	NUM
eurjchem-376	125	34	,	,	PUNCT
eurjchem-376	125	35	2nh	2nh	NOUN
eurjchem-376	125	36	,	,	PUNCT
eurjchem-376	125	37	exchangeable	exchangeable	ADJ
eurjchem-376	125	38	)	)	PUNCT
eurjchem-376	125	39	.	.	PUNCT
eurjchem-376	126	1	anal	anal	PROPN
eurjchem-376	126	2	.	.	PUNCT
eurjchem-376	126	3	calcd	calcd	NOUN
eurjchem-376	126	4	.	.	PUNCT
eurjchem-376	127	1	for	for	ADP
eurjchem-376	127	2	c20h13n5os2	c20h13n5os2	NOUN
eurjchem-376	127	3	:	:	PUNCT
eurjchem-376	127	4	c	c	X
eurjchem-376	127	5	,	,	PUNCT
eurjchem-376	127	6	59.54	59.54	NUM
eurjchem-376	127	7	;	;	PUNCT
eurjchem-376	127	8	h	h	NOUN
eurjchem-376	127	9	,	,	PUNCT
eurjchem-376	127	10	3.25	3.25	NUM
eurjchem-376	127	11	;	;	PUNCT
eurjchem-376	127	12	n	n	CCONJ
eurjchem-376	127	13	,	,	PUNCT
eurjchem-376	127	14	17.36	17.36	NUM
eurjchem-376	127	15	.	.	PUNCT
eurjchem-376	128	1	found	find	VERB
eurjchem-376	128	2	:	:	PUNCT
eurjchem-376	129	1	c	c	X
eurjchem-376	129	2	,	,	PUNCT
eurjchem-376	129	3	59.19	59.19	NUM
eurjchem-376	129	4	;	;	PUNCT
eurjchem-376	129	5	h	h	NOUN
eurjchem-376	129	6	,	,	PUNCT
eurjchem-376	129	7	3.11	3.11	NUM
eurjchem-376	129	8	;	;	PUNCT
eurjchem-376	129	9	n	n	CCONJ
eurjchem-376	129	10	,	,	PUNCT
eurjchem-376	129	11	17.20	17.20	NUM
eurjchem-376	129	12	%	%	NOUN
eurjchem-376	129	13	.	.	PUNCT
eurjchem-376	130	1	2.1.9	2.1.9	NUM
eurjchem-376	130	2	.	.	PUNCT
eurjchem-376	130	3	general	general	ADJ
eurjchem-376	130	4	procedure	procedure	NOUN
eurjchem-376	130	5	for	for	ADP
eurjchem-376	130	6	the	the	DET
eurjchem-376	130	7	synthesis	synthesis	NOUN
eurjchem-376	130	8	of	of	ADP
eurjchem-376	130	9	pyrimidines	pyrimidine	NOUN
eurjchem-376	130	10	(	(	PUNCT
eurjchem-376	130	11	12a‐d	12a‐d	NOUN
eurjchem-376	130	12	)	)	PUNCT
eurjchem-376	130	13	a	a	DET
eurjchem-376	130	14	cold	cold	ADJ
eurjchem-376	130	15	solution	solution	NOUN
eurjchem-376	130	16	of	of	ADP
eurjchem-376	130	17	aryl	aryl	NOUN
eurjchem-376	130	18	diazonium	diazonium	NOUN
eurjchem-376	130	19	chloride	chloride	NOUN
eurjchem-376	130	20	(	(	PUNCT
eurjchem-376	130	21	0.01	0.01	NUM
eurjchem-376	130	22	mol	mol	NOUN
eurjchem-376	130	23	)	)	PUNCT
eurjchem-376	130	24	namely	namely	ADV
eurjchem-376	130	25	benzene	benzene	NOUN
eurjchem-376	130	26	diazonium	diazonium	NOUN
eurjchem-376	130	27	chloride	chloride	NOUN
eurjchem-376	130	28	or	or	CCONJ
eurjchem-376	130	29	4‐methxybenzene	4‐methxybenzene	NUM
eurjchem-376	130	30	diazonium	diazonium	NOUN
eurjchem-376	130	31	chloride	chloride	NOUN
eurjchem-376	130	32	was	be	AUX
eurjchem-376	130	33	added	add	VERB
eurjchem-376	130	34	to	to	ADP
eurjchem-376	130	35	stirred	stir	VERB
eurjchem-376	130	36	solution	solution	NOUN
eurjchem-376	130	37	of	of	ADP
eurjchem-376	130	38	pyrimidines	pyrimidine	NOUN
eurjchem-376	130	39	11a	11a	NOUN
eurjchem-376	130	40	,	,	PUNCT
eurjchem-376	130	41	b	b	PROPN
eurjchem-376	130	42	(	(	PUNCT
eurjchem-376	130	43	0.01	0.01	NUM
eurjchem-376	130	44	mol	mol	NOUN
eurjchem-376	130	45	)	)	PUNCT
eurjchem-376	130	46	in	in	ADP
eurjchem-376	130	47	ethanol	ethanol	NOUN
eurjchem-376	130	48	(	(	PUNCT
eurjchem-376	130	49	30	30	NUM
eurjchem-376	130	50	ml	ml	NOUN
eurjchem-376	130	51	)	)	PUNCT
eurjchem-376	130	52	and	and	CCONJ
eurjchem-376	130	53	sodium	sodium	NOUN
eurjchem-376	130	54	acetate	acetate	NOUN
eurjchem-376	130	55	.	.	PUNCT
eurjchem-376	131	1	the	the	DET
eurjchem-376	131	2	reaction	reaction	NOUN
eurjchem-376	131	3	mixture	mixture	NOUN
eurjchem-376	131	4	was	be	AUX
eurjchem-376	131	5	stirred	stir	VERB
eurjchem-376	131	6	at	at	ADP
eurjchem-376	131	7	room	room	NOUN
eurjchem-376	131	8	temperature	temperature	NOUN
eurjchem-376	131	9	for	for	ADP
eurjchem-376	131	10	3	3	NUM
eurjchem-376	131	11	hours	hour	NOUN
eurjchem-376	131	12	and	and	CCONJ
eurjchem-376	131	13	the	the	DET
eurjchem-376	131	14	formed	form	VERB
eurjchem-376	131	15	solid	solid	ADJ
eurjchem-376	131	16	product	product	NOUN
eurjchem-376	131	17	was	be	AUX
eurjchem-376	131	18	collected	collect	VERB
eurjchem-376	131	19	by	by	ADP
eurjchem-376	131	20	filtration	filtration	NOUN
eurjchem-376	131	21	,	,	PUNCT
eurjchem-376	131	22	washed	wash	VERB
eurjchem-376	131	23	,	,	PUNCT
eurjchem-376	131	24	dried	dry	VERB
eurjchem-376	131	25	and	and	CCONJ
eurjchem-376	131	26	crystallized	crystallize	VERB
eurjchem-376	131	27	from	from	ADP
eurjchem-376	131	28	proper	proper	ADJ
eurjchem-376	131	29	solvent	solvent	NOUN
eurjchem-376	131	30	(	(	PUNCT
eurjchem-376	131	31	scheme	scheme	NOUN
eurjchem-376	131	32	4	4	NUM
eurjchem-376	131	33	)	)	PUNCT
eurjchem-376	131	34	.	.	PUNCT
eurjchem-376	132	1	6‐(6‐dibenzothiophen‐2‐yl	6‐(6‐dibenzothiophen‐2‐yl	PROPN
eurjchem-376	132	2	–	–	PUNCT
eurjchem-376	132	3	pyridazin‐3‐ylamino)‐5‐	pyridazin‐3‐ylamino)‐5‐	NOUN
eurjchem-376	132	4	(	(	PUNCT
eurjchem-376	132	5	phenylhydrazono)pyrimidine‐2,4(3h,5h)‐dione	phenylhydrazono)pyrimidine‐2,4(3h,5h)‐dione	X
eurjchem-376	132	6	(	(	PUNCT
eurjchem-376	132	7	12a	12a	NUM
eurjchem-376	132	8	):	):	PUNCT
eurjchem-376	132	9	yellow	yellow	ADJ
eurjchem-376	132	10	,	,	PUNCT
eurjchem-376	132	11	yield	yield	NOUN
eurjchem-376	132	12	:	:	PUNCT
eurjchem-376	132	13	74	74	NUM
eurjchem-376	132	14	%	%	NOUN
eurjchem-376	132	15	(	(	PUNCT
eurjchem-376	132	16	ethanol	ethanol	NOUN
eurjchem-376	132	17	)	)	PUNCT
eurjchem-376	132	18	.	.	PUNCT
eurjchem-376	133	1	m.p	m.p	PROPN
eurjchem-376	133	2	.	.	PROPN
eurjchem-376	133	3	:	:	PUNCT
eurjchem-376	134	1	191‐193	191‐193	NUM
eurjchem-376	134	2	c	c	ADJ
eurjchem-376	134	3	.	.	PUNCT
eurjchem-376	135	1	ir	ir	PROPN
eurjchem-376	135	2	(	(	PUNCT
eurjchem-376	135	3	kbr	kbr	PROPN
eurjchem-376	135	4	,	,	PUNCT
eurjchem-376	135	5	cm‐1	cm‐1	PROPN
eurjchem-376	135	6	):	):	PUNCT
eurjchem-376	135	7	3435‐	3435‐	NUM
eurjchem-376	135	8	3220	3220	NUM
eurjchem-376	135	9	(oh	(oh	NOUN
eurjchem-376	135	10	,	,	PUNCT
eurjchem-376	135	11	nh	nh	PROPN
eurjchem-376	135	12	)	)	PUNCT
eurjchem-376	135	13	1675	1675	NUM
eurjchem-376	135	14	,	,	PUNCT
eurjchem-376	135	15	1665	1665	NUM
eurjchem-376	135	16	(co	(co	NOUN
eurjchem-376	135	17	)	)	PUNCT
eurjchem-376	135	18	,	,	PUNCT
eurjchem-376	135	19	1620	1620	NUM
eurjchem-376	135	20	(c	(c	PROPN
eurjchem-376	135	21	=	=	SYM
eurjchem-376	135	22	n	n	NUM
eurjchem-376	135	23	)	)	PUNCT
eurjchem-376	135	24	.	.	PUNCT
eurjchem-376	136	1	1h	1h	NUM
eurjchem-376	136	2	nmr	nmr	NOUN
eurjchem-376	136	3	(	(	PUNCT
eurjchem-376	136	4	200	200	NUM
eurjchem-376	136	5	mhz	mhz	NOUN
eurjchem-376	136	6	,	,	PUNCT
eurjchem-376	136	7	cdcl3	cdcl3	NOUN
eurjchem-376	136	8	):	):	PUNCT
eurjchem-376	136	9	5.32	5.32	NUM
eurjchem-376	136	10	,	,	PUNCT
eurjchem-376	136	11	7.21	7.21	NUM
eurjchem-376	136	12	,	,	PUNCT
eurjchem-376	136	13	10.41	10.41	NUM
eurjchem-376	136	14	(	(	PUNCT
eurjchem-376	136	15	3s	3s	NOUN
eurjchem-376	136	16	,	,	PUNCT
eurjchem-376	136	17	3h	3h	NUM
eurjchem-376	136	18	,	,	PUNCT
eurjchem-376	136	19	3nh	3nh	ADJ
eurjchem-376	136	20	,	,	PUNCT
eurjchem-376	136	21	exchangeable	exchangeable	ADJ
eurjchem-376	136	22	)	)	PUNCT
eurjchem-376	136	23	,	,	PUNCT
eurjchem-376	136	24	6.74‐7.93	6.74‐7.93	NUM
eurjchem-376	136	25	(	(	PUNCT
eurjchem-376	136	26	m	m	PROPN
eurjchem-376	136	27	,	,	PUNCT
eurjchem-376	136	28	14h	14h	NUM
eurjchem-376	136	29	,	,	PUNCT
eurjchem-376	136	30	ar‐h	ar‐h	NOUN
eurjchem-376	136	31	)	)	PUNCT
eurjchem-376	136	32	.	.	PUNCT
eurjchem-376	137	1	ms	ms	NOUN
eurjchem-376	137	2	(	(	PUNCT
eurjchem-376	137	3	m	m	PROPN
eurjchem-376	137	4	/	/	SYM
eurjchem-376	137	5	z	z	NOUN
eurjchem-376	137	6	):	):	PUNCT
eurjchem-376	137	7	491	491	NUM
eurjchem-376	137	8	(	(	PUNCT
eurjchem-376	137	9	m+	m+	NUM
eurjchem-376	137	10	)	)	PUNCT
eurjchem-376	137	11	.	.	PUNCT
eurjchem-376	138	1	anal	anal	PROPN
eurjchem-376	138	2	.	.	PUNCT
eurjchem-376	138	3	calcd	calcd	NOUN
eurjchem-376	138	4	.	.	PUNCT
eurjchem-376	139	1	for	for	SCONJ
eurjchem-376	139	2	c26h17n7o2s	c26h17n7o2s	PROPN
eurjchem-376	139	3	:	:	PUNCT
eurjchem-376	139	4	c	c	X
eurjchem-376	139	5	,	,	PUNCT
eurjchem-376	139	6	63.53	63.53	NUM
eurjchem-376	139	7	;	;	PUNCT
eurjchem-376	139	8	h	h	X
eurjchem-376	139	9	,	,	PUNCT
eurjchem-376	139	10	3.49	3.49	NUM
eurjchem-376	139	11	;	;	PUNCT
eurjchem-376	139	12	n	n	CCONJ
eurjchem-376	139	13	,	,	PUNCT
eurjchem-376	139	14	19.95	19.95	NUM
eurjchem-376	139	15	.	.	PUNCT
eurjchem-376	139	16	found	find	VERB
eurjchem-376	139	17	:	:	PUNCT
eurjchem-376	140	1	c	c	X
eurjchem-376	140	2	,	,	PUNCT
eurjchem-376	140	3	63.40	63.40	NUM
eurjchem-376	140	4	;	;	PUNCT
eurjchem-376	140	5	h	h	NOUN
eurjchem-376	140	6	,	,	PUNCT
eurjchem-376	140	7	3.28	3.28	NUM
eurjchem-376	140	8	;	;	PUNCT
eurjchem-376	140	9	n	n	CCONJ
eurjchem-376	140	10	,	,	PUNCT
eurjchem-376	140	11	19.71	19.71	NUM
eurjchem-376	140	12	%	%	NOUN
eurjchem-376	140	13	.	.	PUNCT
eurjchem-376	141	1	6‐(6‐dibenzothiophen‐2‐yl	6‐(6‐dibenzothiophen‐2‐yl	NOUN
eurjchem-376	141	2	–	–	PUNCT
eurjchem-376	141	3	pyridazin‐3‐ylamino)‐5‐(4‐	pyridazin‐3‐ylamino)‐5‐(4‐	NOUN
eurjchem-376	141	4	methoxyphenyl	methoxyphenyl	NOUN
eurjchem-376	141	5	)	)	PUNCT
eurjchem-376	141	6	hydrazonopyrimidine‐2,4(3h,5h)‐dione	hydrazonopyrimidine‐2,4(3h,5h)‐dione	NOUN
eurjchem-376	141	7	(	(	PUNCT
eurjchem-376	141	8	12b	12b	X
eurjchem-376	141	9	):	):	PUNCT
eurjchem-376	141	10	yellow	yellow	ADJ
eurjchem-376	141	11	,	,	PUNCT
eurjchem-376	141	12	yield	yield	NOUN
eurjchem-376	141	13	:	:	PUNCT
eurjchem-376	141	14	77	77	NUM
eurjchem-376	141	15	%	%	NOUN
eurjchem-376	141	16	(	(	PUNCT
eurjchem-376	141	17	ethanol	ethanol	NOUN
eurjchem-376	141	18	)	)	PUNCT
eurjchem-376	141	19	.	.	PUNCT
eurjchem-376	142	1	m.p	m.p	PROPN
eurjchem-376	142	2	.	.	PROPN
eurjchem-376	142	3	:	:	PUNCT
eurjchem-376	142	4	211‐213	211‐213	NUM
eurjchem-376	142	5	c	c	ADJ
eurjchem-376	142	6	.	.	PUNCT
eurjchem-376	143	1	ir	ir	PROPN
eurjchem-376	143	2	(	(	PUNCT
eurjchem-376	143	3	kbr	kbr	PROPN
eurjchem-376	143	4	,	,	PUNCT
eurjchem-376	143	5	cm‐1	cm‐1	PROPN
eurjchem-376	143	6	):	):	PUNCT
eurjchem-376	143	7	3460‐3235	3460‐3235	NUM
eurjchem-376	143	8	(oh	(oh	NOUN
eurjchem-376	143	9	,	,	PUNCT
eurjchem-376	143	10	nh	nh	PROPN
eurjchem-376	143	11	)	)	PUNCT
eurjchem-376	143	12	,	,	PUNCT
eurjchem-376	143	13	1670	1670	NUM
eurjchem-376	143	14	,	,	PUNCT
eurjchem-376	143	15	1665	1665	NUM
eurjchem-376	143	16	(co	(co	NOUN
eurjchem-376	143	17	)	)	PUNCT
eurjchem-376	143	18	,	,	PUNCT
eurjchem-376	143	19	1630	1630	NUM
eurjchem-376	143	20	(c	(c	PROPN
eurjchem-376	143	21	=	=	SYM
eurjchem-376	143	22	n	n	NUM
eurjchem-376	143	23	)	)	PUNCT
eurjchem-376	143	24	.	.	PUNCT
eurjchem-376	144	1	1h	1h	NUM
eurjchem-376	144	2	nmr	nmr	NOUN
eurjchem-376	144	3	(	(	PUNCT
eurjchem-376	144	4	200	200	NUM
eurjchem-376	144	5	mhz	mhz	NOUN
eurjchem-376	144	6	,	,	PUNCT
eurjchem-376	144	7	cdcl3	cdcl3	NOUN
eurjchem-376	144	8	):	):	PUNCT
eurjchem-376	144	9	3.55	3.55	NUM
eurjchem-376	144	10	(	(	PUNCT
eurjchem-376	144	11	s	s	PROPN
eurjchem-376	144	12	,	,	PUNCT
eurjchem-376	144	13	3h	3h	NUM
eurjchem-376	144	14	,	,	PUNCT
eurjchem-376	144	15	och3	och3	ADJ
eurjchem-376	144	16	)	)	PUNCT
eurjchem-376	144	17	,	,	PUNCT
eurjchem-376	144	18	7.44	7.44	NUM
eurjchem-376	144	19	,	,	PUNCT
eurjchem-376	144	20	8.23	8.23	NUM
eurjchem-376	144	21	,	,	PUNCT
eurjchem-376	144	22	9.82	9.82	NUM
eurjchem-376	144	23	(	(	PUNCT
eurjchem-376	144	24	3s	3s	NOUN
eurjchem-376	144	25	,	,	PUNCT
eurjchem-376	144	26	3h	3h	NUM
eurjchem-376	144	27	,	,	PUNCT
eurjchem-376	144	28	3nh	3nh	ADJ
eurjchem-376	144	29	,	,	PUNCT
eurjchem-376	144	30	exchangeable	exchangeable	ADJ
eurjchem-376	144	31	)	)	PUNCT
eurjchem-376	144	32	6.91‐8.03	6.91‐8.03	NUM
eurjchem-376	144	33	(	(	PUNCT
eurjchem-376	144	34	m	m	PROPN
eurjchem-376	144	35	,	,	PUNCT
eurjchem-376	144	36	13h	13h	NOUN
eurjchem-376	144	37	,	,	PUNCT
eurjchem-376	144	38	ar‐h	ar‐h	NOUN
eurjchem-376	144	39	)	)	PUNCT
eurjchem-376	144	40	.	.	PUNCT
eurjchem-376	145	1	ms	ms	NOUN
eurjchem-376	145	2	(	(	PUNCT
eurjchem-376	145	3	m	m	PROPN
eurjchem-376	145	4	/	/	SYM
eurjchem-376	145	5	z	z	NOUN
eurjchem-376	145	6	):	):	PUNCT
eurjchem-376	145	7	521	521	NUM
eurjchem-376	145	8	(	(	PUNCT
eurjchem-376	145	9	m+	m+	NUM
eurjchem-376	145	10	)	)	PUNCT
eurjchem-376	145	11	.	.	PUNCT
eurjchem-376	146	1	anal	anal	PROPN
eurjchem-376	146	2	.	.	PUNCT
eurjchem-376	146	3	calcd	calcd	NOUN
eurjchem-376	146	4	.	.	PUNCT
eurjchem-376	147	1	for	for	SCONJ
eurjchem-376	147	2	c27h19n7o3s	c27h19n7o3s	PROPN
eurjchem-376	147	3	:	:	PUNCT
eurjchem-376	147	4	c	c	X
eurjchem-376	147	5	,	,	PUNCT
eurjchem-376	147	6	62.18	62.18	NUM
eurjchem-376	147	7	;	;	PUNCT
eurjchem-376	147	8	h	h	NOUN
eurjchem-376	147	9	,	,	PUNCT
eurjchem-376	147	10	3.67	3.67	NUM
eurjchem-376	147	11	;	;	PUNCT
eurjchem-376	147	12	n	n	CCONJ
eurjchem-376	147	13	,	,	PUNCT
eurjchem-376	147	14	8.80	8.80	NUM
eurjchem-376	147	15	.	.	PUNCT
eurjchem-376	147	16	found	find	VERB
eurjchem-376	147	17	:	:	PUNCT
eurjchem-376	148	1	c	c	X
eurjchem-376	148	2	,	,	PUNCT
eurjchem-376	148	3	61.88	61.88	NUM
eurjchem-376	148	4	;	;	PUNCT
eurjchem-376	148	5	h	h	NOUN
eurjchem-376	148	6	,	,	PUNCT
eurjchem-376	148	7	3.50	3.50	NUM
eurjchem-376	148	8	;	;	PUNCT
eurjchem-376	148	9	n	n	CCONJ
eurjchem-376	148	10	,	,	PUNCT
eurjchem-376	148	11	8.62	8.62	NUM
eurjchem-376	148	12	%	%	NOUN
eurjchem-376	148	13	.	.	PUNCT
eurjchem-376	149	1	6‐(6‐dibenzothiophen‐2‐yl	6‐(6‐dibenzothiophen‐2‐yl	NOUN
eurjchem-376	149	2	–	–	PUNCT
eurjchem-376	149	3	pyridazin‐3‐ylamino)‐5‐phenyl	pyridazin‐3‐ylamino)‐5‐phenyl	PROPN
eurjchem-376	149	4	hydrazono‐2‐thioxo‐2,3‐dihydropyrimidine‐4(5h)‐one	hydrazono‐2‐thioxo‐2,3‐dihydropyrimidine‐4(5h)‐one	PROPN
eurjchem-376	149	5	(	(	PUNCT
eurjchem-376	149	6	12c	12c	NUM
eurjchem-376	149	7	):	):	PUNCT
eurjchem-376	149	8	yellow	yellow	ADJ
eurjchem-376	149	9	,	,	PUNCT
eurjchem-376	149	10	yield	yield	NOUN
eurjchem-376	149	11	:	:	PUNCT
eurjchem-376	149	12	69	69	NUM
eurjchem-376	149	13	%	%	NOUN
eurjchem-376	149	14	(	(	PUNCT
eurjchem-376	149	15	ethanol	ethanol	NOUN
eurjchem-376	149	16	)	)	PUNCT
eurjchem-376	149	17	.	.	PUNCT
eurjchem-376	150	1	m.p	m.p	PROPN
eurjchem-376	150	2	.	.	PROPN
eurjchem-376	150	3	:	:	PUNCT
eurjchem-376	151	1	217‐219	217‐219	NUM
eurjchem-376	151	2	c	c	ADJ
eurjchem-376	151	3	.	.	PUNCT
eurjchem-376	152	1	ir	ir	PROPN
eurjchem-376	152	2	(	(	PUNCT
eurjchem-376	152	3	kbr	kbr	PROPN
eurjchem-376	152	4	,	,	PUNCT
eurjchem-376	152	5	cm‐1	cm‐1	PROPN
eurjchem-376	152	6	):	):	PUNCT
eurjchem-376	152	7	3410‐3210	3410‐3210	PROPN
eurjchem-376	152	8	(nh	(nh	PROPN
eurjchem-376	152	9	)	)	PUNCT
eurjchem-376	152	10	1680	1680	NUM
eurjchem-376	152	11	,	,	PUNCT
eurjchem-376	152	12	1668	1668	NUM
eurjchem-376	152	13	(co	(co	NOUN
eurjchem-376	152	14	)	)	PUNCT
eurjchem-376	152	15	,	,	PUNCT
eurjchem-376	152	16	1620	1620	NUM
eurjchem-376	152	17	(c	(c	PROPN
eurjchem-376	152	18	=	=	SYM
eurjchem-376	152	19	n	n	NUM
eurjchem-376	152	20	)	)	PUNCT
eurjchem-376	152	21	.	.	PUNCT
eurjchem-376	153	1	1h	1h	NUM
eurjchem-376	153	2	nmr	nmr	NOUN
eurjchem-376	153	3	(	(	PUNCT
eurjchem-376	153	4	200	200	NUM
eurjchem-376	153	5	mhz	mhz	NOUN
eurjchem-376	153	6	,	,	PUNCT
eurjchem-376	153	7	cdcl3	cdcl3	NOUN
eurjchem-376	153	8	):	):	PUNCT
eurjchem-376	153	9	5.63	5.63	NUM
eurjchem-376	153	10	,	,	PUNCT
eurjchem-376	153	11	9.28	9.28	NUM
eurjchem-376	153	12	,	,	PUNCT
eurjchem-376	153	13	9.92	9.92	NUM
eurjchem-376	153	14	(	(	PUNCT
eurjchem-376	153	15	3s	3s	NOUN
eurjchem-376	153	16	,	,	PUNCT
eurjchem-376	153	17	3h	3h	NUM
eurjchem-376	153	18	,	,	PUNCT
eurjchem-376	153	19	3nh	3nh	ADJ
eurjchem-376	153	20	,	,	PUNCT
eurjchem-376	153	21	exchangeable	exchangeable	ADJ
eurjchem-376	153	22	)	)	PUNCT
eurjchem-376	153	23	7.10‐8.04	7.10‐8.04	PROPN
eurjchem-376	153	24	(	(	PUNCT
eurjchem-376	153	25	m	m	PROPN
eurjchem-376	153	26	,	,	PUNCT
eurjchem-376	153	27	14h	14h	NUM
eurjchem-376	153	28	,	,	PUNCT
eurjchem-376	153	29	ar‐h	ar‐h	NOUN
eurjchem-376	153	30	)	)	PUNCT
eurjchem-376	153	31	.	.	PUNCT
eurjchem-376	154	1	ms	ms	NOUN
eurjchem-376	154	2	(	(	PUNCT
eurjchem-376	154	3	m	m	PROPN
eurjchem-376	154	4	/	/	SYM
eurjchem-376	154	5	z	z	NOUN
eurjchem-376	154	6	):	):	PUNCT
eurjchem-376	154	7	507	507	NUM
eurjchem-376	154	8	(	(	PUNCT
eurjchem-376	154	9	m+	m+	NUM
eurjchem-376	154	10	)	)	PUNCT
eurjchem-376	154	11	.	.	PUNCT
eurjchem-376	155	1	anal	anal	PROPN
eurjchem-376	155	2	.	.	PUNCT
eurjchem-376	155	3	calcd	calcd	NOUN
eurjchem-376	155	4	.	.	PUNCT
eurjchem-376	156	1	for	for	ADP
eurjchem-376	156	2	c27h17n7os2	c27h17n7os2	PROPN
eurjchem-376	156	3	:	:	PUNCT
eurjchem-376	156	4	c	c	X
eurjchem-376	156	5	,	,	PUNCT
eurjchem-376	156	6	61.52	61.52	NUM
eurjchem-376	156	7	;	;	PUNCT
eurjchem-376	156	8	h	h	NOUN
eurjchem-376	156	9	,	,	PUNCT
eurjchem-376	156	10	3.38	3.38	NUM
eurjchem-376	156	11	;	;	PUNCT
eurjchem-376	156	12	n	n	CCONJ
eurjchem-376	156	13	,	,	PUNCT
eurjchem-376	156	14	19.32	19.32	NUM
eurjchem-376	156	15	.	.	PUNCT
eurjchem-376	156	16	found	find	VERB
eurjchem-376	156	17	:	:	PUNCT
eurjchem-376	157	1	c	c	X
eurjchem-376	157	2	,	,	PUNCT
eurjchem-376	157	3	61.37	61.37	NUM
eurjchem-376	157	4	;	;	PUNCT
eurjchem-376	157	5	h	h	NOUN
eurjchem-376	157	6	,	,	PUNCT
eurjchem-376	157	7	3.25	3.25	NUM
eurjchem-376	157	8	;	;	PUNCT
eurjchem-376	157	9	n	n	CCONJ
eurjchem-376	157	10	,	,	PUNCT
eurjchem-376	157	11	19.21	19.21	NUM
eurjchem-376	157	12	%	%	NOUN
eurjchem-376	157	13	.	.	PUNCT
eurjchem-376	158	1	6‐(6‐dibenzothiophen‐2‐yl	6‐(6‐dibenzothiophen‐2‐yl	NOUN
eurjchem-376	158	2	–	–	PUNCT
eurjchem-376	158	3	pyridazin‐3‐ylamino)‐5‐(4‐	pyridazin‐3‐ylamino)‐5‐(4‐	NOUN
eurjchem-376	158	4	methoxyphenyl)hydrazono‐2‐thioxo‐2,3‐dihydropyrimidine‐	methoxyphenyl)hydrazono‐2‐thioxo‐2,3‐dihydropyrimidine‐	NOUN
eurjchem-376	158	5	4(5h)‐one	4(5h)‐one	NUM
eurjchem-376	158	6	(	(	PUNCT
eurjchem-376	158	7	12d	12d	NUM
eurjchem-376	158	8	):	):	PUNCT
eurjchem-376	158	9	yellow	yellow	ADJ
eurjchem-376	158	10	,	,	PUNCT
eurjchem-376	158	11	yield	yield	NOUN
eurjchem-376	158	12	:	:	PUNCT
eurjchem-376	158	13	80	80	NUM
eurjchem-376	158	14	%	%	NOUN
eurjchem-376	158	15	(	(	PUNCT
eurjchem-376	158	16	ethanol	ethanol	NOUN
eurjchem-376	158	17	)	)	PUNCT
eurjchem-376	158	18	.	.	PUNCT
eurjchem-376	159	1	m.p	m.p	PROPN
eurjchem-376	159	2	.	.	PROPN
eurjchem-376	159	3	:	:	PUNCT
eurjchem-376	160	1	184‐186	184‐186	NUM
eurjchem-376	160	2	c	c	ADJ
eurjchem-376	160	3	.	.	PUNCT
eurjchem-376	161	1	ir	ir	PROPN
eurjchem-376	161	2	(	(	PUNCT
eurjchem-376	161	3	kbr	kbr	PROPN
eurjchem-376	161	4	,	,	PUNCT
eurjchem-376	161	5	cm‐1	cm‐1	PROPN
eurjchem-376	161	6	):	):	PUNCT
eurjchem-376	161	7	3420‐3190	3420‐3190	NUM
eurjchem-376	161	8	(oh	(oh	NOUN
eurjchem-376	161	9	,	,	PUNCT
eurjchem-376	161	10	nh	nh	PROPN
eurjchem-376	161	11	)	)	PUNCT
eurjchem-376	161	12	,	,	PUNCT
eurjchem-376	161	13	1682	1682	NUM
eurjchem-376	161	14	,	,	PUNCT
eurjchem-376	161	15	1670	1670	NUM
eurjchem-376	161	16	(co	(co	NOUN
eurjchem-376	161	17	)	)	PUNCT
eurjchem-376	161	18	,	,	PUNCT
eurjchem-376	161	19	1626	1626	NUM
eurjchem-376	161	20	(c	(c	NOUN
eurjchem-376	161	21	=	=	SYM
eurjchem-376	161	22	n	n	NUM
eurjchem-376	161	23	)	)	PUNCT
eurjchem-376	161	24	.	.	PUNCT
eurjchem-376	162	1	1h	1h	NUM
eurjchem-376	162	2	nmr	nmr	NOUN
eurjchem-376	162	3	(	(	PUNCT
eurjchem-376	162	4	200	200	NUM
eurjchem-376	162	5	mhz	mhz	NOUN
eurjchem-376	162	6	,	,	PUNCT
eurjchem-376	162	7	cdcl3	cdcl3	NOUN
eurjchem-376	162	8	):	):	PUNCT
eurjchem-376	162	9	3.33	3.33	NUM
eurjchem-376	162	10	(	(	PUNCT
eurjchem-376	162	11	s	s	PROPN
eurjchem-376	162	12	,	,	PUNCT
eurjchem-376	162	13	3h	3h	NUM
eurjchem-376	162	14	,	,	PUNCT
eurjchem-376	162	15	och3	och3	ADJ
eurjchem-376	162	16	)	)	PUNCT
eurjchem-376	162	17	,	,	PUNCT
eurjchem-376	162	18	8.33	8.33	NUM
eurjchem-376	162	19	,	,	PUNCT
eurjchem-376	162	20	8.94	8.94	NUM
eurjchem-376	162	21	,	,	PUNCT
eurjchem-376	162	22	10.40	10.40	NUM
eurjchem-376	162	23	(	(	PUNCT
eurjchem-376	162	24	3s	3s	NOUN
eurjchem-376	162	25	,	,	PUNCT
eurjchem-376	162	26	3h	3h	NUM
eurjchem-376	162	27	,	,	PUNCT
eurjchem-376	162	28	3nh	3nh	ADJ
eurjchem-376	162	29	,	,	PUNCT
eurjchem-376	162	30	exchangeable	exchangeable	ADJ
eurjchem-376	162	31	)	)	PUNCT
eurjchem-376	162	32	6.83‐7.94	6.83‐7.94	NUM
eurjchem-376	162	33	(	(	PUNCT
eurjchem-376	162	34	m	m	PROPN
eurjchem-376	162	35	,	,	PUNCT
eurjchem-376	162	36	13h	13h	NOUN
eurjchem-376	162	37	,	,	PUNCT
eurjchem-376	162	38	ar‐h	ar‐h	NOUN
eurjchem-376	162	39	)	)	PUNCT
eurjchem-376	162	40	.	.	PUNCT
eurjchem-376	163	1	ms	ms	NOUN
eurjchem-376	163	2	(	(	PUNCT
eurjchem-376	163	3	m	m	PROPN
eurjchem-376	163	4	/	/	SYM
eurjchem-376	163	5	z	z	NOUN
eurjchem-376	163	6	):	):	PUNCT
eurjchem-376	163	7	537	537	NUM
eurjchem-376	163	8	(	(	PUNCT
eurjchem-376	163	9	m+	m+	NUM
eurjchem-376	163	10	)	)	PUNCT
eurjchem-376	163	11	.	.	PUNCT
eurjchem-376	164	1	anal	anal	PROPN
eurjchem-376	164	2	.	.	PUNCT
eurjchem-376	164	3	calcd	calcd	NOUN
eurjchem-376	164	4	.	.	PUNCT
eurjchem-376	165	1	for	for	SCONJ
eurjchem-376	165	2	c27h19n7o2s2	c27h19n7o2s2	NOUN
eurjchem-376	165	3	:	:	PUNCT
eurjchem-376	165	4	c	c	X
eurjchem-376	165	5	,	,	PUNCT
eurjchem-376	165	6	60.32	60.32	NUM
eurjchem-376	165	7	;	;	PUNCT
eurjchem-376	165	8	h	h	NOUN
eurjchem-376	165	9	,	,	PUNCT
eurjchem-376	165	10	3.56	3.56	NUM
eurjchem-376	165	11	;	;	PUNCT
eurjchem-376	165	12	n	n	CCONJ
eurjchem-376	165	13	,	,	PUNCT
eurjchem-376	165	14	18.24	18.24	NUM
eurjchem-376	165	15	.	.	PUNCT
eurjchem-376	165	16	found	find	VERB
eurjchem-376	165	17	:	:	PUNCT
eurjchem-376	166	1	c	c	X
eurjchem-376	166	2	,	,	PUNCT
eurjchem-376	166	3	60.24	60.24	NUM
eurjchem-376	166	4	;	;	PUNCT
eurjchem-376	166	5	h	h	NOUN
eurjchem-376	166	6	,	,	PUNCT
eurjchem-376	166	7	3.42	3.42	NUM
eurjchem-376	166	8	;	;	PUNCT
eurjchem-376	166	9	n	n	CCONJ
eurjchem-376	166	10	,	,	PUNCT
eurjchem-376	166	11	18.11	18.11	NUM
eurjchem-376	166	12	%	%	NOUN
eurjchem-376	166	13	.	.	PUNCT
eurjchem-376	167	1	2.1.10	2.1.10	NUM
eurjchem-376	167	2	.	.	PUNCT
eurjchem-376	167	3	general	general	ADJ
eurjchem-376	167	4	procedure	procedure	NOUN
eurjchem-376	167	5	for	for	ADP
eurjchem-376	167	6	the	the	DET
eurjchem-376	167	7	synthesis	synthesis	NOUN
eurjchem-376	167	8	of	of	ADP
eurjchem-376	167	9	pyrimidines	pyrimidine	NOUN
eurjchem-376	167	10	(	(	PUNCT
eurjchem-376	167	11	13a‐d	13a‐d	NOUN
eurjchem-376	167	12	)	)	PUNCT
eurjchem-376	167	13	a	a	DET
eurjchem-376	167	14	mixture	mixture	NOUN
eurjchem-376	167	15	of	of	ADP
eurjchem-376	167	16	pyrimidine	pyrimidine	NOUN
eurjchem-376	167	17	11a	11a	NOUN
eurjchem-376	167	18	,	,	PUNCT
eurjchem-376	167	19	b	b	PROPN
eurjchem-376	167	20	(	(	PUNCT
eurjchem-376	167	21	0.01	0.01	NUM
eurjchem-376	167	22	mol	mol	NOUN
eurjchem-376	167	23	)	)	PUNCT
eurjchem-376	167	24	and	and	CCONJ
eurjchem-376	167	25	aromatic	aromatic	ADJ
eurjchem-376	167	26	aldehydes	aldehyde	NOUN
eurjchem-376	167	27	,	,	PUNCT
eurjchem-376	167	28	e.g.	e.g.	ADV
eurjchem-376	167	29	benzaldehyde	benzaldehyde	NOUN
eurjchem-376	167	30	and	and	CCONJ
eurjchem-376	167	31	4‐chlorobenzaldahyde	4‐chlorobenzaldahyde	NOUN
eurjchem-376	167	32	(	(	PUNCT
eurjchem-376	167	33	0.01	0.01	NUM
eurjchem-376	167	34	mol	mol	NOUN
eurjchem-376	167	35	)	)	PUNCT
eurjchem-376	167	36	was	be	AUX
eurjchem-376	167	37	heated	heat	VERB
eurjchem-376	167	38	in	in	ADP
eurjchem-376	167	39	ethanol	ethanol	NOUN
eurjchem-376	167	40	(	(	PUNCT
eurjchem-376	167	41	30	30	NUM
eurjchem-376	167	42	ml	ml	NOUN
eurjchem-376	167	43	)	)	PUNCT
eurjchem-376	167	44	under	under	ADP
eurjchem-376	167	45	reflux	reflux	NOUN
eurjchem-376	167	46	for	for	ADP
eurjchem-376	167	47	6	6	NUM
eurjchem-376	167	48	hours	hour	NOUN
eurjchem-376	167	49	then	then	ADV
eurjchem-376	167	50	left	leave	VERB
eurjchem-376	167	51	to	to	PART
eurjchem-376	167	52	cool	cool	ADJ
eurjchem-376	167	53	.	.	PUNCT
eurjchem-376	168	1	the	the	DET
eurjchem-376	168	2	solid	solid	ADJ
eurjchem-376	168	3	product	product	NOUN
eurjchem-376	168	4	was	be	AUX
eurjchem-376	168	5	collected	collect	VERB
eurjchem-376	168	6	by	by	ADP
eurjchem-376	168	7	filtration	filtration	NOUN
eurjchem-376	168	8	and	and	CCONJ
eurjchem-376	168	9	recrystallized	recrystallize	VERB
eurjchem-376	168	10	from	from	ADP
eurjchem-376	168	11	proper	proper	ADJ
eurjchem-376	168	12	solvent	solvent	NOUN
eurjchem-376	168	13	(	(	PUNCT
eurjchem-376	168	14	scheme	scheme	NOUN
eurjchem-376	168	15	4	4	NUM
eurjchem-376	168	16	)	)	PUNCT
eurjchem-376	168	17	.	.	PUNCT
eurjchem-376	169	1	5‐benzylidene‐6‐(6‐dibenzothiophen‐2‐yl	5‐benzylidene‐6‐(6‐dibenzothiophen‐2‐yl	NUM
eurjchem-376	169	2	–	–	PUNCT
eurjchem-376	169	3	pyridazin‐3‐	pyridazin‐3‐	NUM
eurjchem-376	169	4	ylamino)pyrimidine‐2,4	ylamino)pyrimidine‐2,4	NOUN
eurjchem-376	169	5	(	(	PUNCT
eurjchem-376	169	6	3h,5h)‐dione	3h,5h)‐dione	NUM
eurjchem-376	169	7	(	(	PUNCT
eurjchem-376	169	8	13a	13a	NOUN
eurjchem-376	169	9	):	):	PUNCT
eurjchem-376	169	10	yellow	yellow	ADJ
eurjchem-376	169	11	,	,	PUNCT
eurjchem-376	169	12	yield	yield	NOUN
eurjchem-376	169	13	:	:	PUNCT
eurjchem-376	169	14	85	85	NUM
eurjchem-376	169	15	%	%	NOUN
eurjchem-376	169	16	(	(	PUNCT
eurjchem-376	169	17	ethanol	ethanol	NOUN
eurjchem-376	169	18	)	)	PUNCT
eurjchem-376	169	19	.	.	PUNCT
eurjchem-376	170	1	m.p	m.p	PROPN
eurjchem-376	170	2	.	.	PROPN
eurjchem-376	170	3	:	:	PUNCT
eurjchem-376	171	1	188‐190	188‐190	PROPN
eurjchem-376	171	2	c	c	VERB
eurjchem-376	171	3	.	.	PUNCT
eurjchem-376	172	1	ir	ir	PROPN
eurjchem-376	172	2	(	(	PUNCT
eurjchem-376	172	3	kbr	kbr	PROPN
eurjchem-376	172	4	,	,	PUNCT
eurjchem-376	172	5	cm‐1	cm‐1	PROPN
eurjchem-376	172	6	):	):	PUNCT
eurjchem-376	172	7	3415‐3140	3415‐3140	NUM
eurjchem-376	172	8	(oh	(oh	NOUN
eurjchem-376	172	9	,	,	PUNCT
eurjchem-376	172	10	nh	nh	PROPN
eurjchem-376	172	11	)	)	PUNCT
eurjchem-376	172	12	1675	1675	NUM
eurjchem-376	172	13	,	,	PUNCT
eurjchem-376	172	14	1667	1667	NUM
eurjchem-376	172	15	(co	(co	NOUN
eurjchem-376	172	16	)	)	PUNCT
eurjchem-376	172	17	,	,	PUNCT
eurjchem-376	172	18	1620	1620	NUM
eurjchem-376	172	19	(c	(c	PROPN
eurjchem-376	172	20	=	=	SYM
eurjchem-376	172	21	n	n	NUM
eurjchem-376	172	22	)	)	PUNCT
eurjchem-376	172	23	,	,	PUNCT
eurjchem-376	172	24	1605	1605	NUM
eurjchem-376	172	25	(c	(c	PROPN
eurjchem-376	172	26	=	=	SYM
eurjchem-376	172	27	c	c	NOUN
eurjchem-376	172	28	)	)	PUNCT
eurjchem-376	172	29	.	.	PUNCT
eurjchem-376	173	1	1h	1h	NUM
eurjchem-376	173	2	nmr	nmr	NOUN
eurjchem-376	173	3	(	(	PUNCT
eurjchem-376	173	4	200	200	NUM
eurjchem-376	173	5	mhz	mhz	NOUN
eurjchem-376	173	6	,	,	PUNCT
eurjchem-376	173	7	cdcl3	cdcl3	NOUN
eurjchem-376	173	8	):	):	PUNCT
eurjchem-376	173	9	8.34	8.34	NUM
eurjchem-376	173	10	,	,	PUNCT
eurjchem-376	173	11	10.13	10.13	NUM
eurjchem-376	173	12	(	(	PUNCT
eurjchem-376	173	13	2s	2s	NUM
eurjchem-376	173	14	,	,	PUNCT
eurjchem-376	173	15	2h	2h	NUM
eurjchem-376	173	16	,	,	PUNCT
eurjchem-376	173	17	2nh	2nh	NOUN
eurjchem-376	173	18	,	,	PUNCT
eurjchem-376	173	19	exchangeable	exchangeable	ADJ
eurjchem-376	173	20	)	)	PUNCT
eurjchem-376	173	21	,	,	PUNCT
eurjchem-376	173	22	6.91‐7.93	6.91‐7.93	NUM
eurjchem-376	173	23	(	(	PUNCT
eurjchem-376	173	24	m	m	PROPN
eurjchem-376	173	25	,	,	PUNCT
eurjchem-376	173	26	15h	15h	NUM
eurjchem-376	173	27	,	,	PUNCT
eurjchem-376	173	28	ar‐h	ar‐h	PROPN
eurjchem-376	173	29	and	and	CCONJ
eurjchem-376	173	30	ch	ch	NOUN
eurjchem-376	173	31	=	=	NOUN
eurjchem-376	173	32	c	c	NOUN
eurjchem-376	173	33	)	)	PUNCT
eurjchem-376	173	34	.	.	PUNCT
eurjchem-376	174	1	ms	ms	NOUN
eurjchem-376	174	2	(	(	PUNCT
eurjchem-376	174	3	m	m	PROPN
eurjchem-376	174	4	/	/	SYM
eurjchem-376	174	5	z	z	NOUN
eurjchem-376	174	6	):	):	PUNCT
eurjchem-376	174	7	475	475	NUM
eurjchem-376	174	8	(	(	PUNCT
eurjchem-376	174	9	m+	m+	NUM
eurjchem-376	174	10	)	)	PUNCT
eurjchem-376	174	11	.	.	PUNCT
eurjchem-376	175	1	anal	anal	PROPN
eurjchem-376	175	2	.	.	PUNCT
eurjchem-376	175	3	calcd	calcd	NOUN
eurjchem-376	175	4	.	.	PUNCT
eurjchem-376	176	1	for	for	SCONJ
eurjchem-376	176	2	c27h17n5o2s	c27h17n5o2s	PROPN
eurjchem-376	176	3	:	:	PUNCT
eurjchem-376	176	4	c	c	X
eurjchem-376	176	5	,	,	PUNCT
eurjchem-376	176	6	68.20	68.20	NUM
eurjchem-376	176	7	;	;	PUNCT
eurjchem-376	176	8	h	h	NOUN
eurjchem-376	176	9	,	,	PUNCT
eurjchem-376	176	10	3.60	3.60	NUM
eurjchem-376	176	11	;	;	PUNCT
eurjchem-376	176	12	n	n	CCONJ
eurjchem-376	176	13	,	,	PUNCT
eurjchem-376	176	14	14.73	14.73	NUM
eurjchem-376	176	15	.	.	PUNCT
eurjchem-376	176	16	found	find	VERB
eurjchem-376	176	17	:	:	PUNCT
eurjchem-376	177	1	c	c	X
eurjchem-376	177	2	,	,	PUNCT
eurjchem-376	177	3	68.03	68.03	NUM
eurjchem-376	177	4	;	;	PUNCT
eurjchem-376	177	5	h	h	NOUN
eurjchem-376	177	6	,	,	PUNCT
eurjchem-376	177	7	3.48	3.48	NUM
eurjchem-376	177	8	;	;	PUNCT
eurjchem-376	177	9	n	n	CCONJ
eurjchem-376	177	10	,	,	PUNCT
eurjchem-376	177	11	14.57	14.57	NUM
eurjchem-376	177	12	%	%	NOUN
eurjchem-376	177	13	.	.	PUNCT
eurjchem-376	178	1	5‐(4‐chlorobenzylidene)‐6‐(6‐dibenzothiophen‐2‐yl	5‐(4‐chlorobenzylidene)‐6‐(6‐dibenzothiophen‐2‐yl	NUM
eurjchem-376	178	2	–	–	PUNCT
eurjchem-376	178	3	pyridazin‐3‐ylamino)pyrimidine‐2,4(3h,5h)‐dione	pyridazin‐3‐ylamino)pyrimidine‐2,4(3h,5h)‐dione	NOUN
eurjchem-376	178	4	(	(	PUNCT
eurjchem-376	178	5	13b	13b	NUM
eurjchem-376	178	6	):	):	PUNCT
eurjchem-376	178	7	yellow	yellow	ADJ
eurjchem-376	178	8	yield	yield	NOUN
eurjchem-376	178	9	:	:	PUNCT
eurjchem-376	178	10	87	87	NUM
eurjchem-376	178	11	%	%	NOUN
eurjchem-376	178	12	(	(	PUNCT
eurjchem-376	178	13	ethanol	ethanol	NOUN
eurjchem-376	178	14	)	)	PUNCT
eurjchem-376	178	15	.	.	PUNCT
eurjchem-376	179	1	m.p	m.p	PROPN
eurjchem-376	179	2	.	.	PROPN
eurjchem-376	179	3	:	:	PUNCT
eurjchem-376	179	4	167‐169	167‐169	NUM
eurjchem-376	179	5	c	c	ADJ
eurjchem-376	179	6	.	.	PUNCT
eurjchem-376	180	1	ir	ir	PROPN
eurjchem-376	180	2	(	(	PUNCT
eurjchem-376	180	3	kbr	kbr	PROPN
eurjchem-376	180	4	,	,	PUNCT
eurjchem-376	180	5	cm‐1	cm‐1	PROPN
eurjchem-376	180	6	):	):	PUNCT
eurjchem-376	180	7	3400‐	3400‐	NUM
eurjchem-376	180	8	3175	3175	NUM
eurjchem-376	180	9	(oh	(oh	NOUN
eurjchem-376	180	10	,	,	PUNCT
eurjchem-376	180	11	nh	nh	PROPN
eurjchem-376	180	12	)	)	PUNCT
eurjchem-376	180	13	,	,	PUNCT
eurjchem-376	180	14	1681	1681	NUM
eurjchem-376	180	15	,	,	PUNCT
eurjchem-376	180	16	1668	1668	NUM
eurjchem-376	180	17	(co	(co	NOUN
eurjchem-376	180	18	)	)	PUNCT
eurjchem-376	180	19	,	,	PUNCT
eurjchem-376	180	20	1625	1625	NUM
eurjchem-376	180	21	(c	(c	NOUN
eurjchem-376	180	22	=	=	SYM
eurjchem-376	180	23	n),1616	n),1616	ADJ
eurjchem-376	180	24	(c	(c	NOUN
eurjchem-376	180	25	=	=	SYM
eurjchem-376	180	26	c	c	NOUN
eurjchem-376	180	27	)	)	PUNCT
eurjchem-376	180	28	.	.	PUNCT
eurjchem-376	181	1	1h	1h	NUM
eurjchem-376	181	2	nmr	nmr	NOUN
eurjchem-376	181	3	(	(	PUNCT
eurjchem-376	181	4	200	200	NUM
eurjchem-376	181	5	mhz	mhz	NOUN
eurjchem-376	181	6	,	,	PUNCT
eurjchem-376	181	7	cdcl3	cdcl3	NOUN
eurjchem-376	181	8	):	):	PUNCT
eurjchem-376	181	9	9.24	9.24	NUM
eurjchem-376	181	10	,	,	PUNCT
eurjchem-376	181	11	10.61	10.61	NUM
eurjchem-376	181	12	(	(	PUNCT
eurjchem-376	181	13	2s	2s	NUM
eurjchem-376	181	14	,	,	PUNCT
eurjchem-376	181	15	2h	2h	NUM
eurjchem-376	181	16	,	,	PUNCT
eurjchem-376	181	17	2nh	2nh	NOUN
eurjchem-376	181	18	,	,	PUNCT
eurjchem-376	181	19	exchangeable	exchangeable	ADJ
eurjchem-376	181	20	)	)	PUNCT
eurjchem-376	181	21	,	,	PUNCT
eurjchem-376	181	22	7.10‐8.22	7.10‐8.22	NUM
eurjchem-376	181	23	(	(	PUNCT
eurjchem-376	181	24	m	m	PROPN
eurjchem-376	181	25	,	,	PUNCT
eurjchem-376	181	26	14h	14h	NUM
eurjchem-376	181	27	,	,	PUNCT
eurjchem-376	181	28	ar‐h	ar‐h	NOUN
eurjchem-376	181	29	and	and	CCONJ
eurjchem-376	181	30	ch	ch	NOUN
eurjchem-376	181	31	=	=	NOUN
eurjchem-376	181	32	c	c	NOUN
eurjchem-376	181	33	)	)	PUNCT
eurjchem-376	181	34	.	.	PUNCT
eurjchem-376	182	1	anal	anal	PROPN
eurjchem-376	182	2	.	.	PUNCT
eurjchem-376	182	3	calcd	calcd	NOUN
eurjchem-376	182	4	.	.	PUNCT
eurjchem-376	183	1	for	for	ADP
eurjchem-376	183	2	c27h16cln5o2s	c27h16cln5o2s	NOUN
eurjchem-376	183	3	:	:	PUNCT
eurjchem-376	183	4	c	c	X
eurjchem-376	183	5	,	,	PUNCT
eurjchem-376	183	6	63.59	63.59	NUM
eurjchem-376	183	7	;	;	PUNCT
eurjchem-376	183	8	h	h	NOUN
eurjchem-376	183	9	,	,	PUNCT
eurjchem-376	183	10	3.16	3.16	NUM
eurjchem-376	183	11	;	;	PUNCT
eurjchem-376	183	12	n	n	CCONJ
eurjchem-376	183	13	,	,	PUNCT
eurjchem-376	183	14	13.73	13.73	NUM
eurjchem-376	183	15	.	.	PUNCT
eurjchem-376	183	16	found	find	VERB
eurjchem-376	183	17	:	:	PUNCT
eurjchem-376	184	1	c	c	X
eurjchem-376	184	2	,	,	PUNCT
eurjchem-376	184	3	63.43	63.43	NUM
eurjchem-376	184	4	;	;	PUNCT
eurjchem-376	184	5	h	h	NOUN
eurjchem-376	184	6	,	,	PUNCT
eurjchem-376	184	7	3.06	3.06	NUM
eurjchem-376	184	8	;	;	PUNCT
eurjchem-376	184	9	n	n	CCONJ
eurjchem-376	184	10	,	,	PUNCT
eurjchem-376	184	11	13.57	13.57	NUM
eurjchem-376	184	12	%	%	NOUN
eurjchem-376	184	13	.	.	PUNCT
eurjchem-376	185	1	5‐benzylidene‐6‐(6‐dibenzothiophen‐2‐yl	5‐benzylidene‐6‐(6‐dibenzothiophen‐2‐yl	NUM
eurjchem-376	185	2	–	–	PUNCT
eurjchem-376	185	3	pyridazin‐3‐yl	pyridazin‐3‐yl	NOUN
eurjchem-376	185	4	amino)‐2‐thioxo‐2,3‐dihydropyrimidine‐4(5h)‐one	amino)‐2‐thioxo‐2,3‐dihydropyrimidine‐4(5h)‐one	NOUN
eurjchem-376	185	5	(	(	PUNCT
eurjchem-376	185	6	13c	13c	X
eurjchem-376	185	7	):	):	PUNCT
eurjchem-376	185	8	yellow	yellow	ADJ
eurjchem-376	185	9	,	,	PUNCT
eurjchem-376	185	10	yield	yield	NOUN
eurjchem-376	185	11	:	:	PUNCT
eurjchem-376	185	12	78	78	NUM
eurjchem-376	185	13	%	%	NOUN
eurjchem-376	185	14	(	(	PUNCT
eurjchem-376	185	15	ethanol	ethanol	NOUN
eurjchem-376	185	16	)	)	PUNCT
eurjchem-376	185	17	.	.	PUNCT
eurjchem-376	186	1	m.p	m.p	PROPN
eurjchem-376	186	2	.	.	PROPN
eurjchem-376	186	3	:	:	PUNCT
eurjchem-376	187	1	182‐184	182‐184	X
eurjchem-376	187	2	c	c	VERB
eurjchem-376	187	3	.	.	PUNCT
eurjchem-376	188	1	ir	ir	PROPN
eurjchem-376	188	2	(	(	PUNCT
eurjchem-376	188	3	kbr	kbr	PROPN
eurjchem-376	188	4	,	,	PUNCT
eurjchem-376	188	5	cm‐1	cm‐1	PROPN
eurjchem-376	188	6	):	):	PUNCT
eurjchem-376	188	7	3480‐3160	3480‐3160	NUM
eurjchem-376	188	8	(oh	(oh	NOUN
eurjchem-376	188	9	,	,	PUNCT
eurjchem-376	188	10	nh	nh	PROPN
eurjchem-376	188	11	)	)	PUNCT
eurjchem-376	188	12	,	,	PUNCT
eurjchem-376	188	13	1680	1680	NUM
eurjchem-376	188	14	,	,	PUNCT
eurjchem-376	188	15	1665	1665	NUM
eurjchem-376	188	16	(co	(co	NOUN
eurjchem-376	188	17	)	)	PUNCT
eurjchem-376	188	18	,	,	PUNCT
eurjchem-376	188	19	1625	1625	NUM
eurjchem-376	188	20	(c	(c	PROPN
eurjchem-376	188	21	=	=	SYM
eurjchem-376	188	22	n	n	CCONJ
eurjchem-376	188	23	)	)	PUNCT
eurjchem-376	188	24	,	,	PUNCT
eurjchem-376	188	25	1612	1612	NUM
eurjchem-376	188	26	(c	(c	PROPN
eurjchem-376	188	27	=	=	SYM
eurjchem-376	188	28	c	c	NOUN
eurjchem-376	188	29	)	)	PUNCT
eurjchem-376	188	30	.	.	PUNCT
eurjchem-376	189	1	1h	1h	NUM
eurjchem-376	189	2	nmr	nmr	NOUN
eurjchem-376	189	3	(	(	PUNCT
eurjchem-376	189	4	200	200	NUM
eurjchem-376	189	5	mhz	mhz	NOUN
eurjchem-376	189	6	,	,	PUNCT
eurjchem-376	189	7	cdcl3	cdcl3	NOUN
eurjchem-376	189	8	):	):	PUNCT
eurjchem-376	189	9	8.51	8.51	NUM
eurjchem-376	189	10	,	,	PUNCT
eurjchem-376	189	11	9.87	9.87	NUM
eurjchem-376	189	12	(	(	PUNCT
eurjchem-376	189	13	2s	2s	NUM
eurjchem-376	189	14	,	,	PUNCT
eurjchem-376	189	15	2h	2h	NUM
eurjchem-376	189	16	,	,	PUNCT
eurjchem-376	189	17	2nh	2nh	NOUN
eurjchem-376	189	18	,	,	PUNCT
eurjchem-376	189	19	exchangeable	exchangeable	ADJ
eurjchem-376	189	20	)	)	PUNCT
eurjchem-376	189	21	,	,	PUNCT
eurjchem-376	189	22	6.84‐7.92	6.84‐7.92	NUM
eurjchem-376	189	23	(	(	PUNCT
eurjchem-376	189	24	m	m	PROPN
eurjchem-376	189	25	,	,	PUNCT
eurjchem-376	189	26	15h	15h	NUM
eurjchem-376	189	27	,	,	PUNCT
eurjchem-376	189	28	ar‐h	ar‐h	PROPN
eurjchem-376	189	29	and	and	CCONJ
eurjchem-376	189	30	ch	ch	NOUN
eurjchem-376	189	31	=	=	NOUN
eurjchem-376	189	32	c	c	NOUN
eurjchem-376	189	33	)	)	PUNCT
eurjchem-376	189	34	.	.	PUNCT
eurjchem-376	190	1	anal	anal	PROPN
eurjchem-376	190	2	.	.	PUNCT
eurjchem-376	190	3	calcd	calcd	NOUN
eurjchem-376	190	4	.	.	PUNCT
eurjchem-376	191	1	for	for	SCONJ
eurjchem-376	191	2	c27h17n5o2s	c27h17n5o2s	PROPN
eurjchem-376	191	3	:	:	PUNCT
eurjchem-376	191	4	c	c	X
eurjchem-376	191	5	,	,	PUNCT
eurjchem-376	191	6	65.97	65.97	NUM
eurjchem-376	191	7	;	;	PUNCT
eurjchem-376	191	8	h	h	NOUN
eurjchem-376	191	9	,	,	PUNCT
eurjchem-376	191	10	3.49	3.49	NUM
eurjchem-376	191	11	;	;	PUNCT
eurjchem-376	191	12	n	n	CCONJ
eurjchem-376	191	13	,	,	PUNCT
eurjchem-376	191	14	14.25	14.25	NUM
eurjchem-376	191	15	.	.	PUNCT
eurjchem-376	191	16	found	find	VERB
eurjchem-376	191	17	:	:	PUNCT
eurjchem-376	192	1	c	c	X
eurjchem-376	192	2	,	,	PUNCT
eurjchem-376	192	3	65.75	65.75	NUM
eurjchem-376	192	4	;	;	PUNCT
eurjchem-376	192	5	h	h	NOUN
eurjchem-376	192	6	,	,	PUNCT
eurjchem-376	192	7	3.33	3.33	NUM
eurjchem-376	192	8	;	;	PUNCT
eurjchem-376	192	9	n	n	DET
eurjchem-376	192	10	14.11	14.11	NUM
eurjchem-376	192	11	%	%	NOUN
eurjchem-376	192	12	.	.	PUNCT
eurjchem-376	193	1	5‐(4‐chlorobenzylidene)‐6‐(6‐dibenzothiophen‐2‐yl	5‐(4‐chlorobenzylidene)‐6‐(6‐dibenzothiophen‐2‐yl	ADJ
eurjchem-376	193	2	–	–	PUNCT
eurjchem-376	193	3	pyridazin‐3‐ylamino)‐2‐thioxo‐2,3‐dihydropyrimidine‐4(5h)‐one	pyridazin‐3‐ylamino)‐2‐thioxo‐2,3‐dihydropyrimidine‐4(5h)‐one	NOUN
eurjchem-376	193	4	(	(	PUNCT
eurjchem-376	193	5	13d	13d	NUM
eurjchem-376	193	6	):	):	PUNCT
eurjchem-376	193	7	yellow	yellow	ADJ
eurjchem-376	193	8	,	,	PUNCT
eurjchem-376	193	9	yield	yield	NOUN
eurjchem-376	193	10	:	:	PUNCT
eurjchem-376	193	11	81	81	NUM
eurjchem-376	193	12	%	%	NOUN
eurjchem-376	193	13	(	(	PUNCT
eurjchem-376	193	14	ethanol	ethanol	NOUN
eurjchem-376	193	15	)	)	PUNCT
eurjchem-376	193	16	.	.	PUNCT
eurjchem-376	194	1	m.p	m.p	PROPN
eurjchem-376	194	2	.	.	PROPN
eurjchem-376	194	3	:	:	PUNCT
eurjchem-376	195	1	202‐204	202‐204	NUM
eurjchem-376	195	2	c	c	ADJ
eurjchem-376	195	3	.	.	PUNCT
eurjchem-376	196	1	ir	ir	PROPN
eurjchem-376	196	2	(	(	PUNCT
eurjchem-376	196	3	kbr	kbr	PROPN
eurjchem-376	196	4	,	,	PUNCT
eurjchem-376	196	5	cm‐1	cm‐1	PROPN
eurjchem-376	196	6	):	):	PUNCT
eurjchem-376	196	7	3455‐3215	3455‐3215	NUM
eurjchem-376	196	8	(oh	(oh	NOUN
eurjchem-376	196	9	,	,	PUNCT
eurjchem-376	196	10	nh	nh	PROPN
eurjchem-376	196	11	)	)	PUNCT
eurjchem-376	196	12	,	,	PUNCT
eurjchem-376	196	13	1675	1675	NUM
eurjchem-376	196	14	,	,	PUNCT
eurjchem-376	196	15	1662	1662	NUM
eurjchem-376	196	16	(co	(co	NOUN
eurjchem-376	196	17	)	)	PUNCT
eurjchem-376	196	18	,	,	PUNCT
eurjchem-376	196	19	1625	1625	NUM
eurjchem-376	196	20	(c	(c	PROPN
eurjchem-376	196	21	=	=	SYM
eurjchem-376	196	22	n	n	NUM
eurjchem-376	196	23	)	)	PUNCT
eurjchem-376	196	24	,	,	PUNCT
eurjchem-376	196	25	1610	1610	NUM
eurjchem-376	196	26	(c	(c	NOUN
eurjchem-376	196	27	=	=	SYM
eurjchem-376	196	28	c	c	NOUN
eurjchem-376	196	29	)	)	PUNCT
eurjchem-376	196	30	.	.	PUNCT
eurjchem-376	197	1	1h	1h	NUM
eurjchem-376	197	2	nmr	nmr	NOUN
eurjchem-376	197	3	(	(	PUNCT
eurjchem-376	197	4	200	200	NUM
eurjchem-376	197	5	mhz	mhz	NOUN
eurjchem-376	197	6	,	,	PUNCT
eurjchem-376	197	7	cdcl3	cdcl3	NOUN
eurjchem-376	197	8	):	):	PUNCT
eurjchem-376	197	9	9.37	9.37	NUM
eurjchem-376	197	10	,	,	PUNCT
eurjchem-376	197	11	10.21	10.21	NUM
eurjchem-376	197	12	(	(	PUNCT
eurjchem-376	197	13	2s	2s	NUM
eurjchem-376	197	14	,	,	PUNCT
eurjchem-376	197	15	2h	2h	NUM
eurjchem-376	197	16	,	,	PUNCT
eurjchem-376	197	17	2nh	2nh	NOUN
eurjchem-376	197	18	,	,	PUNCT
eurjchem-376	197	19	exchangeable	exchangeable	ADJ
eurjchem-376	197	20	)	)	PUNCT
eurjchem-376	197	21	,	,	PUNCT
eurjchem-376	197	22	6.90‐8.11(m	6.90‐8.11(m	NUM
eurjchem-376	197	23	,	,	PUNCT
eurjchem-376	197	24	14h	14h	NUM
eurjchem-376	197	25	,	,	PUNCT
eurjchem-376	197	26	ar‐h	ar‐h	NOUN
eurjchem-376	197	27	and	and	CCONJ
eurjchem-376	197	28	ch	ch	NOUN
eurjchem-376	197	29	=	=	NOUN
eurjchem-376	197	30	c	c	NOUN
eurjchem-376	197	31	)	)	PUNCT
eurjchem-376	197	32	.	.	PUNCT
eurjchem-376	198	1	anal	anal	PROPN
eurjchem-376	198	2	.	.	PUNCT
eurjchem-376	198	3	calcd	calcd	NOUN
eurjchem-376	198	4	.	.	PUNCT
eurjchem-376	199	1	for	for	SCONJ
eurjchem-376	199	2	c27h16cln5o2s	c27h16cln5o2s	NOUN
eurjchem-376	199	3	:	:	PUNCT
eurjchem-376	199	4	c	c	X
eurjchem-376	199	5	,	,	PUNCT
eurjchem-376	199	6	61.65	61.65	NUM
eurjchem-376	199	7	;	;	PUNCT
eurjchem-376	199	8	h	h	NOUN
eurjchem-376	199	9	,	,	PUNCT
eurjchem-376	199	10	3.07	3.07	NUM
eurjchem-376	199	11	;	;	PUNCT
eurjchem-376	199	12	n	n	CCONJ
eurjchem-376	199	13	,	,	PUNCT
eurjchem-376	199	14	13.31	13.31	NUM
eurjchem-376	199	15	.	.	PUNCT
eurjchem-376	199	16	found	find	VERB
eurjchem-376	199	17	:	:	PUNCT
eurjchem-376	200	1	c	c	X
eurjchem-376	200	2	,	,	PUNCT
eurjchem-376	200	3	61.71	61.71	NUM
eurjchem-376	200	4	;	;	PUNCT
eurjchem-376	200	5	h	h	NOUN
eurjchem-376	200	6	,	,	PUNCT
eurjchem-376	200	7	3.16	3.16	NUM
eurjchem-376	200	8	;	;	PUNCT
eurjchem-376	200	9	n	n	CCONJ
eurjchem-376	200	10	,	,	PUNCT
eurjchem-376	200	11	13.19	13.19	NUM
eurjchem-376	200	12	%	%	NOUN
eurjchem-376	200	13	.	.	PUNCT
eurjchem-376	201	1	298	298	NUM
eurjchem-376	201	2	behalo	behalo	NOUN
eurjchem-376	201	3	and	and	CCONJ
eurjchem-376	201	4	aly	aly	PROPN
eurjchem-376	201	5	/	/	SYM
eurjchem-376	201	6	european	european	PROPN
eurjchem-376	201	7	journal	journal	PROPN
eurjchem-376	201	8	of	of	ADP
eurjchem-376	201	9	chemistry	chemistry	NOUN
eurjchem-376	201	10	2	2	NUM
eurjchem-376	201	11	(	(	PUNCT
eurjchem-376	201	12	3	3	NUM
eurjchem-376	201	13	)	)	PUNCT
eurjchem-376	201	14	(	(	PUNCT
eurjchem-376	201	15	2011	2011	NUM
eurjchem-376	201	16	)	)	PUNCT
eurjchem-376	201	17	295‐299	295‐299	NOUN
eurjchem-376	201	18	scheme	scheme	NOUN
eurjchem-376	201	19	4	4	NUM
eurjchem-376	201	20	2.1.11	2.1.11	NUM
eurjchem-376	201	21	.	.	PUNCT
eurjchem-376	202	1	general	general	ADJ
eurjchem-376	202	2	procedure	procedure	NOUN
eurjchem-376	202	3	for	for	ADP
eurjchem-376	202	4	the	the	DET
eurjchem-376	202	5	synthesis	synthesis	NOUN
eurjchem-376	202	6	of	of	ADP
eurjchem-376	202	7	pyridines	pyridine	NOUN
eurjchem-376	202	8	(	(	PUNCT
eurjchem-376	202	9	14a	14a	NOUN
eurjchem-376	202	10	,	,	PUNCT
eurjchem-376	202	11	b	b	NOUN
eurjchem-376	202	12	)	)	PUNCT
eurjchem-376	202	13	to	to	ADP
eurjchem-376	202	14	a	a	DET
eurjchem-376	202	15	solution	solution	NOUN
eurjchem-376	202	16	of	of	ADP
eurjchem-376	202	17	ester	ester	NOUN
eurjchem-376	202	18	2	2	NUM
eurjchem-376	202	19	(	(	PUNCT
eurjchem-376	202	20	0.01	0.01	NUM
eurjchem-376	202	21	mol	mol	NOUN
eurjchem-376	202	22	)	)	PUNCT
eurjchem-376	202	23	in	in	ADP
eurjchem-376	202	24	dimethylformamide	dimethylformamide	NOUN
eurjchem-376	202	25	(	(	PUNCT
eurjchem-376	202	26	30	30	NUM
eurjchem-376	202	27	ml	ml	NOUN
eurjchem-376	202	28	)	)	PUNCT
eurjchem-376	202	29	containing	contain	VERB
eurjchem-376	202	30	triethylamine	triethylamine	NOUN
eurjchem-376	202	31	(	(	PUNCT
eurjchem-376	202	32	few	few	ADJ
eurjchem-376	202	33	drops	drop	NOUN
eurjchem-376	202	34	)	)	PUNCT
eurjchem-376	202	35	,	,	PUNCT
eurjchem-376	202	36	either	either	CCONJ
eurjchem-376	202	37	malononitrile	malononitrile	NOUN
eurjchem-376	202	38	or	or	CCONJ
eurjchem-376	202	39	ethyl	ethyl	PROPN
eurjchem-376	202	40	cyanoacetate	cyanoacetate	NOUN
eurjchem-376	202	41	(	(	PUNCT
eurjchem-376	202	42	0.01	0.01	NUM
eurjchem-376	202	43	mol	mol	NOUN
eurjchem-376	202	44	)	)	PUNCT
eurjchem-376	202	45	was	be	AUX
eurjchem-376	202	46	added	add	VERB
eurjchem-376	202	47	.	.	PUNCT
eurjchem-376	203	1	after	after	ADP
eurjchem-376	203	2	heating	heating	NOUN
eurjchem-376	203	3	of	of	ADP
eurjchem-376	203	4	the	the	DET
eurjchem-376	203	5	reaction	reaction	NOUN
eurjchem-376	203	6	mixture	mixture	NOUN
eurjchem-376	203	7	for	for	ADP
eurjchem-376	203	8	6	6	NUM
eurjchem-376	203	9	hours	hour	NOUN
eurjchem-376	203	10	and	and	CCONJ
eurjchem-376	203	11	cooling	cooling	NOUN
eurjchem-376	203	12	,	,	PUNCT
eurjchem-376	203	13	the	the	DET
eurjchem-376	203	14	mixture	mixture	NOUN
eurjchem-376	203	15	was	be	AUX
eurjchem-376	203	16	poured	pour	VERB
eurjchem-376	203	17	into	into	ADP
eurjchem-376	203	18	crushed	crushed	ADJ
eurjchem-376	203	19	ice	ice	NOUN
eurjchem-376	203	20	and	and	CCONJ
eurjchem-376	203	21	hydrochloric	hydrochloric	ADJ
eurjchem-376	203	22	acid	acid	NOUN
eurjchem-376	203	23	.	.	PUNCT
eurjchem-376	204	1	the	the	DET
eurjchem-376	204	2	precipitated	precipitate	VERB
eurjchem-376	204	3	product	product	NOUN
eurjchem-376	204	4	was	be	AUX
eurjchem-376	204	5	collected	collect	VERB
eurjchem-376	204	6	by	by	ADP
eurjchem-376	204	7	filtration	filtration	NOUN
eurjchem-376	204	8	,	,	PUNCT
eurjchem-376	204	9	washed	wash	VERB
eurjchem-376	204	10	and	and	CCONJ
eurjchem-376	204	11	dried	dry	VERB
eurjchem-376	204	12	(	(	PUNCT
eurjchem-376	204	13	scheme	scheme	NOUN
eurjchem-376	204	14	5	5	NUM
eurjchem-376	204	15	)	)	PUNCT
eurjchem-376	204	16	.	.	PUNCT
eurjchem-376	205	1	ethyl	ethyl	PROPN
eurjchem-376	205	2	4,6‐diamino‐1‐(6‐dibenzothiophen‐2‐yl‐pyridazin‐3‐	4,6‐diamino‐1‐(6‐dibenzothiophen‐2‐yl‐pyridazin‐3‐	NUM
eurjchem-376	205	3	yl)‐2‐oxo‐1,2‐dihydropyridine‐3‐carboxylate	yl)‐2‐oxo‐1,2‐dihydropyridine‐3‐carboxylate	NOUN
eurjchem-376	205	4	(	(	PUNCT
eurjchem-376	205	5	14a	14a	NOUN
eurjchem-376	205	6	):	):	PUNCT
eurjchem-376	205	7	yellow	yellow	ADJ
eurjchem-376	205	8	,	,	PUNCT
eurjchem-376	205	9	yield	yield	NOUN
eurjchem-376	205	10	:	:	PUNCT
eurjchem-376	205	11	63	63	NUM
eurjchem-376	205	12	%	%	NOUN
eurjchem-376	205	13	(	(	PUNCT
eurjchem-376	205	14	ethanol	ethanol	NOUN
eurjchem-376	205	15	)	)	PUNCT
eurjchem-376	205	16	.	.	PUNCT
eurjchem-376	206	1	m.p	m.p	PROPN
eurjchem-376	206	2	.	.	PROPN
eurjchem-376	206	3	:	:	PUNCT
eurjchem-376	207	1	195‐197	195‐197	NUM
eurjchem-376	207	2	c	c	ADJ
eurjchem-376	207	3	.	.	PUNCT
eurjchem-376	208	1	ir	ir	PROPN
eurjchem-376	208	2	(	(	PUNCT
eurjchem-376	208	3	kbr	kbr	PROPN
eurjchem-376	208	4	,	,	PUNCT
eurjchem-376	208	5	cm‐1	cm‐1	PROPN
eurjchem-376	208	6	):	):	PUNCT
eurjchem-376	208	7	3390‐	3390‐	NUM
eurjchem-376	208	8	3180	3180	NUM
eurjchem-376	208	9	(nh2	(nh2	PROPN
eurjchem-376	208	10	)	)	PUNCT
eurjchem-376	208	11	,	,	PUNCT
eurjchem-376	208	12	3050	3050	NUM
eurjchem-376	208	13	(ch‐aromatic	(ch‐aromatic	NOUN
eurjchem-376	208	14	)	)	PUNCT
eurjchem-376	208	15	,	,	PUNCT
eurjchem-376	208	16	1705	1705	NUM
eurjchem-376	208	17	,	,	PUNCT
eurjchem-376	208	18	1680	1680	NUM
eurjchem-376	208	19	(co	(co	NOUN
eurjchem-376	208	20	)	)	PUNCT
eurjchem-376	208	21	,	,	PUNCT
eurjchem-376	208	22	1620	1620	NUM
eurjchem-376	208	23	(c	(c	PROPN
eurjchem-376	208	24	=	=	SYM
eurjchem-376	208	25	c	c	NOUN
eurjchem-376	208	26	)	)	PUNCT
eurjchem-376	208	27	.	.	PUNCT
eurjchem-376	209	1	1h	1h	NUM
eurjchem-376	209	2	nmr	nmr	NOUN
eurjchem-376	209	3	(	(	PUNCT
eurjchem-376	209	4	200	200	NUM
eurjchem-376	209	5	mhz	mhz	NOUN
eurjchem-376	209	6	,	,	PUNCT
eurjchem-376	209	7	cdcl3	cdcl3	NOUN
eurjchem-376	209	8	):	):	PUNCT
eurjchem-376	209	9	1.31	1.31	NUM
eurjchem-376	209	10	(	(	PUNCT
eurjchem-376	209	11	t	t	PROPN
eurjchem-376	209	12	,	,	PUNCT
eurjchem-376	209	13	3h	3h	NUM
eurjchem-376	209	14	,	,	PUNCT
eurjchem-376	209	15	ch3	ch3	PROPN
eurjchem-376	209	16	)	)	PUNCT
eurjchem-376	209	17	,	,	PUNCT
eurjchem-376	209	18	4.23	4.23	NUM
eurjchem-376	209	19	(	(	PUNCT
eurjchem-376	209	20	q	q	NOUN
eurjchem-376	209	21	,	,	PUNCT
eurjchem-376	209	22	2h	2h	NUM
eurjchem-376	209	23	,	,	PUNCT
eurjchem-376	209	24	ch2	ch2	PROPN
eurjchem-376	209	25	)	)	PUNCT
eurjchem-376	209	26	,	,	PUNCT
eurjchem-376	209	27	6.92‐7.87	6.92‐7.87	NUM
eurjchem-376	209	28	(	(	PUNCT
eurjchem-376	209	29	m	m	PROPN
eurjchem-376	209	30	,	,	PUNCT
eurjchem-376	209	31	9h	9h	NUM
eurjchem-376	209	32	,	,	PUNCT
eurjchem-376	209	33	ar‐h	ar‐h	NOUN
eurjchem-376	209	34	)	)	PUNCT
eurjchem-376	209	35	,	,	PUNCT
eurjchem-376	209	36	7.11	7.11	NUM
eurjchem-376	209	37	(	(	PUNCT
eurjchem-376	209	38	s	s	PROPN
eurjchem-376	209	39	,	,	PUNCT
eurjchem-376	209	40	1h	1h	NUM
eurjchem-376	209	41	,	,	PUNCT
eurjchem-376	209	42	pyridine	pyridine	ADJ
eurjchem-376	209	43	h	h	NOUN
eurjchem-376	209	44	)	)	PUNCT
eurjchem-376	209	45	,	,	PUNCT
eurjchem-376	209	46	8.44	8.44	NUM
eurjchem-376	209	47	,	,	PUNCT
eurjchem-376	209	48	8.93	8.93	NUM
eurjchem-376	209	49	(	(	PUNCT
eurjchem-376	209	50	2s	2s	PROPN
eurjchem-376	209	51	,	,	PUNCT
eurjchem-376	209	52	4h	4h	NUM
eurjchem-376	209	53	,	,	PUNCT
eurjchem-376	209	54	2nh2	2nh2	NUM
eurjchem-376	209	55	,	,	PUNCT
eurjchem-376	209	56	exchangeable	exchangeable	ADJ
eurjchem-376	209	57	)	)	PUNCT
eurjchem-376	209	58	.	.	PUNCT
eurjchem-376	210	1	ms	ms	NOUN
eurjchem-376	210	2	(	(	PUNCT
eurjchem-376	210	3	m	m	PROPN
eurjchem-376	210	4	/	/	SYM
eurjchem-376	210	5	z	z	NOUN
eurjchem-376	210	6	):	):	PUNCT
eurjchem-376	210	7	457	457	NUM
eurjchem-376	210	8	(	(	PUNCT
eurjchem-376	210	9	m+	m+	NUM
eurjchem-376	210	10	)	)	PUNCT
eurjchem-376	210	11	.	.	PUNCT
eurjchem-376	211	1	anal	anal	PROPN
eurjchem-376	211	2	.	.	PUNCT
eurjchem-376	211	3	calcd	calcd	NOUN
eurjchem-376	211	4	.	.	PUNCT
eurjchem-376	212	1	for	for	ADP
eurjchem-376	212	2	c24h19n5o3s	c24h19n5o3s	NUM
eurjchem-376	212	3	:	:	PUNCT
eurjchem-376	212	4	c	c	X
eurjchem-376	212	5	,	,	PUNCT
eurjchem-376	212	6	63.01	63.01	NUM
eurjchem-376	212	7	;	;	PUNCT
eurjchem-376	212	8	h	h	NOUN
eurjchem-376	212	9	,	,	PUNCT
eurjchem-376	212	10	4.19	4.19	NUM
eurjchem-376	212	11	;	;	PUNCT
eurjchem-376	212	12	n	n	CCONJ
eurjchem-376	212	13	,	,	PUNCT
eurjchem-376	212	14	15.31	15.31	NUM
eurjchem-376	212	15	.	.	PUNCT
eurjchem-376	212	16	found	find	VERB
eurjchem-376	212	17	:	:	PUNCT
eurjchem-376	213	1	c	c	X
eurjchem-376	213	2	,	,	PUNCT
eurjchem-376	213	3	62.88	62.88	NUM
eurjchem-376	213	4	;	;	PUNCT
eurjchem-376	213	5	h	h	NOUN
eurjchem-376	213	6	,	,	PUNCT
eurjchem-376	213	7	4.05	4.05	NUM
eurjchem-376	213	8	;	;	PUNCT
eurjchem-376	213	9	n	n	CCONJ
eurjchem-376	213	10	,	,	PUNCT
eurjchem-376	213	11	15.15	15.15	NUM
eurjchem-376	213	12	%	%	NOUN
eurjchem-376	213	13	.	.	PUNCT
eurjchem-376	214	1	ethyl	ethyl	PROPN
eurjchem-376	215	1	4‐amino‐1‐(6‐dibenzothiophen‐2‐yl‐pyridazin‐3‐yl)‐6‐	4‐amino‐1‐(6‐dibenzothiophen‐2‐yl‐pyridazin‐3‐yl)‐6‐	NUM
eurjchem-376	215	2	hydroxy‐2‐oxo‐1,2‐dihydropyridine‐3‐carboxylate	hydroxy‐2‐oxo‐1,2‐dihydropyridine‐3‐carboxylate	NOUN
eurjchem-376	215	3	(	(	PUNCT
eurjchem-376	215	4	14b	14b	NUM
eurjchem-376	215	5	):	):	PUNCT
eurjchem-376	215	6	yellow	yellow	ADJ
eurjchem-376	215	7	,	,	PUNCT
eurjchem-376	215	8	yield	yield	NOUN
eurjchem-376	215	9	:	:	PUNCT
eurjchem-376	215	10	65	65	NUM
eurjchem-376	215	11	%	%	NOUN
eurjchem-376	215	12	(	(	PUNCT
eurjchem-376	215	13	ethanol	ethanol	NOUN
eurjchem-376	215	14	)	)	PUNCT
eurjchem-376	215	15	.	.	PUNCT
eurjchem-376	216	1	m.p	m.p	PROPN
eurjchem-376	216	2	.	.	PROPN
eurjchem-376	216	3	:	:	PUNCT
eurjchem-376	217	1	186‐188	186‐188	NUM
eurjchem-376	217	2	c	c	ADJ
eurjchem-376	217	3	.	.	PUNCT
eurjchem-376	218	1	ir	ir	PROPN
eurjchem-376	218	2	(	(	PUNCT
eurjchem-376	218	3	kbr	kbr	PROPN
eurjchem-376	218	4	,	,	PUNCT
eurjchem-376	218	5	cm‐1	cm‐1	PROPN
eurjchem-376	218	6	):	):	PUNCT
eurjchem-376	218	7	3520‐	3520‐	NUM
eurjchem-376	218	8	3310	3310	NUM
eurjchem-376	218	9	(oh	(oh	NOUN
eurjchem-376	218	10	,	,	PUNCT
eurjchem-376	218	11	nh2	nh2	PROPN
eurjchem-376	218	12	)	)	PUNCT
eurjchem-376	218	13	,	,	PUNCT
eurjchem-376	218	14	3040	3040	NUM
eurjchem-376	218	15	(ch‐aromatic	(ch‐aromatic	NOUN
eurjchem-376	218	16	)	)	PUNCT
eurjchem-376	218	17	,	,	PUNCT
eurjchem-376	218	18	1700	1700	NUM
eurjchem-376	218	19	,	,	PUNCT
eurjchem-376	218	20	1683	1683	NUM
eurjchem-376	218	21	(co	(co	NOUN
eurjchem-376	218	22	)	)	PUNCT
eurjchem-376	218	23	,	,	PUNCT
eurjchem-376	218	24	1626	1626	NUM
eurjchem-376	218	25	(c	(c	NOUN
eurjchem-376	218	26	=	=	SYM
eurjchem-376	218	27	c	c	NOUN
eurjchem-376	218	28	)	)	PUNCT
eurjchem-376	218	29	.	.	PUNCT
eurjchem-376	219	1	1h	1h	NUM
eurjchem-376	219	2	nmr	nmr	NOUN
eurjchem-376	219	3	(	(	PUNCT
eurjchem-376	219	4	200	200	NUM
eurjchem-376	219	5	mhz	mhz	NOUN
eurjchem-376	219	6	,	,	PUNCT
eurjchem-376	219	7	cdcl3	cdcl3	NOUN
eurjchem-376	219	8	):	):	PUNCT
eurjchem-376	219	9	1.29	1.29	NUM
eurjchem-376	219	10	(	(	PUNCT
eurjchem-376	219	11	t	t	PROPN
eurjchem-376	219	12	,	,	PUNCT
eurjchem-376	219	13	3h	3h	NUM
eurjchem-376	219	14	,	,	PUNCT
eurjchem-376	219	15	ch3	ch3	PROPN
eurjchem-376	219	16	)	)	PUNCT
eurjchem-376	219	17	,	,	PUNCT
eurjchem-376	219	18	4.31(q	4.31(q	NOUN
eurjchem-376	219	19	,	,	PUNCT
eurjchem-376	219	20	2h	2h	NUM
eurjchem-376	219	21	,	,	PUNCT
eurjchem-376	219	22	ch2	ch2	PROPN
eurjchem-376	219	23	)	)	PUNCT
eurjchem-376	219	24	,	,	PUNCT
eurjchem-376	219	25	6.98‐7.92	6.98‐7.92	NUM
eurjchem-376	219	26	(	(	PUNCT
eurjchem-376	219	27	m	m	PROPN
eurjchem-376	219	28	,	,	PUNCT
eurjchem-376	219	29	9h	9h	NUM
eurjchem-376	219	30	,	,	PUNCT
eurjchem-376	219	31	ar‐h	ar‐h	NOUN
eurjchem-376	219	32	)	)	PUNCT
eurjchem-376	219	33	,	,	PUNCT
eurjchem-376	219	34	6.91	6.91	NUM
eurjchem-376	219	35	(	(	PUNCT
eurjchem-376	219	36	s	s	PROPN
eurjchem-376	219	37	,	,	PUNCT
eurjchem-376	219	38	1h	1h	NUM
eurjchem-376	219	39	,	,	PUNCT
eurjchem-376	219	40	pyridine	pyridine	ADJ
eurjchem-376	219	41	h	h	NOUN
eurjchem-376	219	42	)	)	PUNCT
eurjchem-376	219	43	,	,	PUNCT
eurjchem-376	219	44	6.33	6.33	NUM
eurjchem-376	219	45	(	(	PUNCT
eurjchem-376	219	46	s	s	PROPN
eurjchem-376	219	47	,	,	PUNCT
eurjchem-376	219	48	2h	2h	NUM
eurjchem-376	219	49	,	,	PUNCT
eurjchem-376	219	50	nh2	nh2	PROPN
eurjchem-376	219	51	,	,	PUNCT
eurjchem-376	219	52	exchangeable	exchangeable	ADJ
eurjchem-376	219	53	)	)	PUNCT
eurjchem-376	219	54	,	,	PUNCT
eurjchem-376	219	55	9.82	9.82	NUM
eurjchem-376	219	56	(	(	PUNCT
eurjchem-376	219	57	s	s	PROPN
eurjchem-376	219	58	,	,	PUNCT
eurjchem-376	219	59	1h	1h	NUM
eurjchem-376	219	60	,	,	PUNCT
eurjchem-376	219	61	oh	oh	INTJ
eurjchem-376	219	62	)	)	PUNCT
eurjchem-376	219	63	.	.	PUNCT
eurjchem-376	220	1	anal	anal	PROPN
eurjchem-376	220	2	.	.	PUNCT
eurjchem-376	220	3	calcd	calcd	NOUN
eurjchem-376	220	4	.	.	PUNCT
eurjchem-376	221	1	for	for	ADP
eurjchem-376	221	2	c24h18n4o4s	c24h18n4o4s	PROPN
eurjchem-376	221	3	:	:	PUNCT
eurjchem-376	221	4	c	c	X
eurjchem-376	221	5	,	,	PUNCT
eurjchem-376	221	6	62.87	62.87	NUM
eurjchem-376	221	7	;	;	PUNCT
eurjchem-376	221	8	h	h	X
eurjchem-376	221	9	,	,	PUNCT
eurjchem-376	221	10	3.96	3.96	NUM
eurjchem-376	221	11	;	;	PUNCT
eurjchem-376	221	12	n	n	CCONJ
eurjchem-376	221	13	,	,	PUNCT
eurjchem-376	221	14	12.22	12.22	NUM
eurjchem-376	221	15	.	.	PUNCT
eurjchem-376	221	16	found	find	VERB
eurjchem-376	221	17	:	:	PUNCT
eurjchem-376	222	1	c	c	X
eurjchem-376	222	2	,	,	PUNCT
eurjchem-376	222	3	62.33	62.33	NUM
eurjchem-376	222	4	;	;	PUNCT
eurjchem-376	222	5	h	h	NOUN
eurjchem-376	222	6	,	,	PUNCT
eurjchem-376	222	7	3.85	3.85	NUM
eurjchem-376	222	8	;	;	PUNCT
eurjchem-376	222	9	n	n	CCONJ
eurjchem-376	222	10	,	,	PUNCT
eurjchem-376	222	11	12.11	12.11	NUM
eurjchem-376	222	12	%	%	NOUN
eurjchem-376	222	13	.	.	PUNCT
eurjchem-376	223	1	2.1.12	2.1.12	X
eurjchem-376	223	2	.	.	PUNCT
eurjchem-376	223	3	ethyl	ethyl	PROPN
eurjchem-376	223	4	6‐amino‐5‐cyano‐1‐(6‐dibenzothiophen‐2‐yl‐	6‐amino‐5‐cyano‐1‐(6‐dibenzothiophen‐2‐yl‐	NUM
eurjchem-376	223	5	pyridazin‐3‐yl)‐2‐oxo‐4‐phenyl‐1,2‐dihydro	pyridazin‐3‐yl)‐2‐oxo‐4‐phenyl‐1,2‐dihydro	NOUN
eurjchem-376	223	6	pyridine‐3‐	pyridine‐3‐	NOUN
eurjchem-376	223	7	carboxylate	carboxylate	NOUN
eurjchem-376	223	8	(	(	PUNCT
eurjchem-376	223	9	15	15	NUM
eurjchem-376	223	10	)	)	PUNCT
eurjchem-376	223	11	the	the	DET
eurjchem-376	223	12	same	same	ADJ
eurjchem-376	223	13	procedures	procedure	NOUN
eurjchem-376	223	14	described	describe	VERB
eurjchem-376	223	15	for	for	ADP
eurjchem-376	223	16	the	the	DET
eurjchem-376	223	17	synthesis	synthesis	NOUN
eurjchem-376	223	18	of	of	ADP
eurjchem-376	223	19	compounds	compound	NOUN
eurjchem-376	223	20	14a	14a	NOUN
eurjchem-376	223	21	,	,	PUNCT
eurjchem-376	223	22	b.	b.	PROPN
eurjchem-376	223	23	yellow	yellow	PROPN
eurjchem-376	223	24	,	,	PUNCT
eurjchem-376	223	25	yield	yield	NOUN
eurjchem-376	223	26	:	:	PUNCT
eurjchem-376	223	27	68	68	NUM
eurjchem-376	223	28	%	%	NOUN
eurjchem-376	223	29	(	(	PUNCT
eurjchem-376	223	30	ethanol	ethanol	NOUN
eurjchem-376	223	31	)	)	PUNCT
eurjchem-376	223	32	(	(	PUNCT
eurjchem-376	223	33	scheme	scheme	NOUN
eurjchem-376	223	34	5	5	NUM
eurjchem-376	223	35	)	)	PUNCT
eurjchem-376	223	36	.	.	PUNCT
eurjchem-376	224	1	m.p	m.p	PROPN
eurjchem-376	224	2	.	.	PROPN
eurjchem-376	224	3	:	:	PUNCT
eurjchem-376	225	1	201‐203	201‐203	NUM
eurjchem-376	225	2	c	c	ADJ
eurjchem-376	225	3	.	.	PUNCT
eurjchem-376	226	1	ir	ir	PROPN
eurjchem-376	226	2	(	(	PUNCT
eurjchem-376	226	3	kbr	kbr	PROPN
eurjchem-376	226	4	,	,	PUNCT
eurjchem-376	226	5	cm‐1	cm‐1	PROPN
eurjchem-376	226	6	):	):	PUNCT
eurjchem-376	226	7	3385‐3190	3385‐3190	NUM
eurjchem-376	226	8	(nh2	(nh2	NOUN
eurjchem-376	226	9	)	)	PUNCT
eurjchem-376	226	10	,	,	PUNCT
eurjchem-376	226	11	3040	3040	NUM
eurjchem-376	226	12	(ch‐aromatic	(ch‐aromatic	NOUN
eurjchem-376	226	13	)	)	PUNCT
eurjchem-376	226	14	,	,	PUNCT
eurjchem-376	226	15	2220	2220	NUM
eurjchem-376	226	16	(c≡n	(c≡n	NOUN
eurjchem-376	226	17	)	)	PUNCT
eurjchem-376	226	18	,	,	PUNCT
eurjchem-376	226	19	1705	1705	NUM
eurjchem-376	226	20	,	,	PUNCT
eurjchem-376	226	21	1685	1685	NUM
eurjchem-376	226	22	(co	(co	NOUN
eurjchem-376	226	23	)	)	PUNCT
eurjchem-376	226	24	,	,	PUNCT
eurjchem-376	226	25	1630	1630	NUM
eurjchem-376	226	26	(c	(c	PROPN
eurjchem-376	226	27	=	=	SYM
eurjchem-376	226	28	c	c	NOUN
eurjchem-376	226	29	)	)	PUNCT
eurjchem-376	226	30	.	.	PUNCT
eurjchem-376	227	1	1h	1h	NUM
eurjchem-376	227	2	nmr	nmr	NOUN
eurjchem-376	227	3	(	(	PUNCT
eurjchem-376	227	4	200	200	NUM
eurjchem-376	227	5	mhz	mhz	NOUN
eurjchem-376	227	6	,	,	PUNCT
eurjchem-376	227	7	cdcl3	cdcl3	NOUN
eurjchem-376	227	8	):	):	PUNCT
eurjchem-376	227	9	1.31	1.31	NUM
eurjchem-376	227	10	(	(	PUNCT
eurjchem-376	227	11	t	t	PROPN
eurjchem-376	227	12	,	,	PUNCT
eurjchem-376	227	13	3h	3h	NUM
eurjchem-376	227	14	,	,	PUNCT
eurjchem-376	227	15	ch3	ch3	PROPN
eurjchem-376	227	16	)	)	PUNCT
eurjchem-376	227	17	,	,	PUNCT
eurjchem-376	227	18	4.32	4.32	NUM
eurjchem-376	227	19	(	(	PUNCT
eurjchem-376	227	20	q	q	NOUN
eurjchem-376	227	21	,	,	PUNCT
eurjchem-376	227	22	2h	2h	NUM
eurjchem-376	227	23	,	,	PUNCT
eurjchem-376	227	24	ch2	ch2	PROPN
eurjchem-376	227	25	)	)	PUNCT
eurjchem-376	227	26	,	,	PUNCT
eurjchem-376	227	27	6.80‐7.93	6.80‐7.93	NUM
eurjchem-376	227	28	(	(	PUNCT
eurjchem-376	227	29	m	m	PROPN
eurjchem-376	227	30	,	,	PUNCT
eurjchem-376	227	31	14h	14h	NUM
eurjchem-376	227	32	,	,	PUNCT
eurjchem-376	227	33	ar‐h	ar‐h	NOUN
eurjchem-376	227	34	)	)	PUNCT
eurjchem-376	227	35	,	,	PUNCT
eurjchem-376	227	36	8.34	8.34	NUM
eurjchem-376	227	37	(	(	PUNCT
eurjchem-376	227	38	s	s	PROPN
eurjchem-376	227	39	,	,	PUNCT
eurjchem-376	227	40	2h	2h	NUM
eurjchem-376	227	41	,	,	PUNCT
eurjchem-376	227	42	nh2	nh2	PROPN
eurjchem-376	227	43	,	,	PUNCT
eurjchem-376	227	44	exchangeable	exchangeable	ADJ
eurjchem-376	227	45	)	)	PUNCT
eurjchem-376	227	46	.	.	PUNCT
eurjchem-376	228	1	anal	anal	PROPN
eurjchem-376	228	2	.	.	PUNCT
eurjchem-376	228	3	calcd	calcd	NOUN
eurjchem-376	228	4	.	.	PUNCT
eurjchem-376	229	1	for	for	ADP
eurjchem-376	229	2	c31h21n5o3s	c31h21n5o3s	NUM
eurjchem-376	229	3	:	:	PUNCT
eurjchem-376	229	4	c	c	X
eurjchem-376	229	5	,	,	PUNCT
eurjchem-376	229	6	68.49	68.49	NUM
eurjchem-376	229	7	;	;	PUNCT
eurjchem-376	229	8	h	h	NOUN
eurjchem-376	229	9	,	,	PUNCT
eurjchem-376	229	10	3.89	3.89	NUM
eurjchem-376	229	11	;	;	PUNCT
eurjchem-376	229	12	n	n	CCONJ
eurjchem-376	229	13	,	,	PUNCT
eurjchem-376	229	14	12.88	12.88	NUM
eurjchem-376	229	15	.	.	PUNCT
eurjchem-376	229	16	found	find	VERB
eurjchem-376	229	17	:	:	PUNCT
eurjchem-376	230	1	c	c	X
eurjchem-376	230	2	,	,	PUNCT
eurjchem-376	230	3	68.36	68.36	NUM
eurjchem-376	230	4	;	;	PUNCT
eurjchem-376	230	5	h	h	NOUN
eurjchem-376	230	6	,	,	PUNCT
eurjchem-376	230	7	3.81	3.81	NUM
eurjchem-376	230	8	;	;	PUNCT
eurjchem-376	230	9	n	n	CCONJ
eurjchem-376	230	10	,	,	PUNCT
eurjchem-376	230	11	12.73	12.73	NUM
eurjchem-376	230	12	%	%	NOUN
eurjchem-376	230	13	.	.	PUNCT
eurjchem-376	231	1	2.2	2.2	NUM
eurjchem-376	231	2	.	.	PUNCT
eurjchem-376	232	1	instrumentation	instrumentation	NOUN
eurjchem-376	232	2	melting	melt	VERB
eurjchem-376	232	3	points	point	NOUN
eurjchem-376	232	4	of	of	ADP
eurjchem-376	232	5	the	the	DET
eurjchem-376	232	6	prepared	prepare	VERB
eurjchem-376	232	7	products	product	NOUN
eurjchem-376	232	8	are	be	AUX
eurjchem-376	232	9	uncorrected	uncorrecte	VERB
eurjchem-376	232	10	.	.	PUNCT
eurjchem-376	233	1	all	all	DET
eurjchem-376	233	2	reactions	reaction	NOUN
eurjchem-376	233	3	were	be	AUX
eurjchem-376	233	4	monitored	monitor	VERB
eurjchem-376	233	5	by	by	ADP
eurjchem-376	233	6	thin	thin	ADJ
eurjchem-376	233	7	layer	layer	NOUN
eurjchem-376	233	8	chromatography	chromatography	NOUN
eurjchem-376	233	9	(	(	PUNCT
eurjchem-376	233	10	tlc	tlc	NOUN
eurjchem-376	233	11	)	)	PUNCT
eurjchem-376	233	12	carried	carry	VERB
eurjchem-376	233	13	out	out	ADP
eurjchem-376	233	14	on	on	ADP
eurjchem-376	233	15	0.2	0.2	NUM
eurjchem-376	233	16	mm	mm	NOUN
eurjchem-376	233	17	silica	silica	NOUN
eurjchem-376	233	18	gel	gel	NOUN
eurjchem-376	233	19	60	60	NUM
eurjchem-376	233	20	f254	f254	PROPN
eurjchem-376	233	21	(	(	PUNCT
eurjchem-376	233	22	merck	merck	NOUN
eurjchem-376	233	23	)	)	PUNCT
eurjchem-376	233	24	plates	plate	NOUN
eurjchem-376	233	25	.	.	PUNCT
eurjchem-376	234	1	ir	ir	PROPN
eurjchem-376	234	2	spectra	spectra	PROPN
eurjchem-376	234	3	in	in	ADP
eurjchem-376	234	4	kbr	kbr	PROPN
eurjchem-376	234	5	were	be	AUX
eurjchem-376	234	6	recorded	record	VERB
eurjchem-376	234	7	using	use	VERB
eurjchem-376	234	8	a	a	DET
eurjchem-376	234	9	perkin‐elmer	perkin‐elmer	NOUN
eurjchem-376	234	10	298	298	NUM
eurjchem-376	234	11	spectrophotometer	spectrophotometer	NOUN
eurjchem-376	234	12	.	.	PUNCT
eurjchem-376	235	1	1h‐	1h‐	NUM
eurjchem-376	235	2	and	and	CCONJ
eurjchem-376	235	3	13c	13c	NOUN
eurjchem-376	235	4	nmr	nmr	NOUN
eurjchem-376	235	5	spectra	spectra	NOUN
eurjchem-376	235	6	were	be	AUX
eurjchem-376	235	7	obtained	obtain	VERB
eurjchem-376	235	8	using	use	VERB
eurjchem-376	235	9	a	a	DET
eurjchem-376	235	10	varian	varian	PROPN
eurjchem-376	235	11	gemini	gemini	PROPN
eurjchem-376	235	12	200	200	NUM
eurjchem-376	235	13	mhz	mhz	NOUN
eurjchem-376	235	14	and	and	CCONJ
eurjchem-376	235	15	50	50	NUM
eurjchem-376	235	16	mhz	mhz	NOUN
eurjchem-376	235	17	instrument	instrument	NOUN
eurjchem-376	235	18	.	.	PUNCT
eurjchem-376	236	1	the	the	DET
eurjchem-376	236	2	solvent	solvent	NOUN
eurjchem-376	236	3	used	use	VERB
eurjchem-376	236	4	for	for	ADP
eurjchem-376	236	5	nmr	nmr	NOUN
eurjchem-376	236	6	analysis	analysis	NOUN
eurjchem-376	236	7	was	be	AUX
eurjchem-376	236	8	cdcl3	cdcl3	NOUN
eurjchem-376	236	9	,	,	PUNCT
eurjchem-376	236	10	unless	unless	SCONJ
eurjchem-376	236	11	stated	state	VERB
eurjchem-376	236	12	otherwise	otherwise	ADV
eurjchem-376	236	13	.	.	PUNCT
eurjchem-376	237	1	mass	mass	PROPN
eurjchem-376	237	2	spectra	spectra	PROPN
eurjchem-376	237	3	were	be	AUX
eurjchem-376	237	4	obtained	obtain	VERB
eurjchem-376	237	5	using	use	VERB
eurjchem-376	237	6	a	a	DET
eurjchem-376	237	7	shimadzu	shimadzu	ADJ
eurjchem-376	237	8	gcms‐qp	gcms‐qp	ADJ
eurjchem-376	237	9	1000	1000	NUM
eurjchem-376	237	10	ex	ex	PRON
eurjchem-376	237	11	mass	mass	NOUN
eurjchem-376	237	12	spectrometer	spectrometer	NOUN
eurjchem-376	237	13	.	.	PUNCT
eurjchem-376	238	1	3	3	X
eurjchem-376	238	2	.	.	NOUN
eurjchem-376	238	3	results	result	NOUN
eurjchem-376	238	4	and	and	CCONJ
eurjchem-376	238	5	discussion	discussion	NOUN
eurjchem-376	238	6	schemes	scheme	NOUN
eurjchem-376	238	7	1‐5	1‐5	PROPN
eurjchem-376	238	8	show	show	VERB
eurjchem-376	238	9	the	the	DET
eurjchem-376	238	10	synthetic	synthetic	ADJ
eurjchem-376	238	11	pathways	pathway	NOUN
eurjchem-376	238	12	to	to	PART
eurjchem-376	238	13	prepare	prepare	VERB
eurjchem-376	238	14	the	the	DET
eurjchem-376	238	15	target	target	NOUN
eurjchem-376	238	16	compounds	compound	VERB
eurjchem-376	238	17	2‐15	2‐15	NUM
eurjchem-376	238	18	.	.	PUNCT
eurjchem-376	239	1	the	the	DET
eurjchem-376	239	2	key	key	ADJ
eurjchem-376	239	3	substrate	substrate	NOUN
eurjchem-376	239	4	ester	ester	NOUN
eurjchem-376	239	5	2	2	NUM
eurjchem-376	239	6	was	be	AUX
eurjchem-376	239	7	synthesized	synthesize	VERB
eurjchem-376	239	8	from	from	ADP
eurjchem-376	239	9	the	the	DET
eurjchem-376	239	10	reaction	reaction	NOUN
eurjchem-376	239	11	of	of	ADP
eurjchem-376	239	12	aminopyridazine	aminopyridazine	NOUN
eurjchem-376	239	13	derivative	derivative	NOUN
eurjchem-376	239	14	[	[	X
eurjchem-376	239	15	25	25	NUM
eurjchem-376	239	16	]	]	SYM
eurjchem-376	239	17	1	1	NUM
eurjchem-376	239	18	and	and	CCONJ
eurjchem-376	239	19	diethyl	diethyl	NOUN
eurjchem-376	239	20	malonate	malonate	NOUN
eurjchem-376	239	21	(	(	PUNCT
eurjchem-376	239	22	scheme	scheme	NOUN
eurjchem-376	239	23	1	1	NUM
eurjchem-376	239	24	)	)	PUNCT
eurjchem-376	239	25	.	.	PUNCT
eurjchem-376	240	1	the	the	DET
eurjchem-376	240	2	ir	ir	PROPN
eurjchem-376	240	3	spectrum	spectrum	NOUN
eurjchem-376	240	4	of	of	ADP
eurjchem-376	240	5	compound	compound	NOUN
eurjchem-376	240	6	2	2	NUM
eurjchem-376	240	7	showed	show	VERB
eurjchem-376	240	8	two	two	NUM
eurjchem-376	240	9	strong	strong	ADJ
eurjchem-376	240	10	absorption	absorption	NOUN
eurjchem-376	240	11	bands	band	NOUN
eurjchem-376	240	12	at	at	ADP
eurjchem-376	240	13	1730	1730	NUM
eurjchem-376	240	14	and	and	CCONJ
eurjchem-376	240	15	1685	1685	NUM
eurjchem-376	240	16	cm‐1	cm‐1	NOUN
eurjchem-376	240	17	assigned	assign	VERB
eurjchem-376	240	18	to	to	ADP
eurjchem-376	240	19	ester	ester	NOUN
eurjchem-376	240	20	and	and	CCONJ
eurjchem-376	240	21	amide	amide	NOUN
eurjchem-376	240	22	carbonyl	carbonyl	NOUN
eurjchem-376	240	23	groups	group	NOUN
eurjchem-376	240	24	respectively	respectively	ADV
eurjchem-376	240	25	.	.	PUNCT
eurjchem-376	241	1	another	another	DET
eurjchem-376	241	2	band	band	NOUN
eurjchem-376	241	3	was	be	AUX
eurjchem-376	241	4	revealed	reveal	VERB
eurjchem-376	241	5	at	at	ADP
eurjchem-376	241	6	3380‐3280	3380‐3280	NUM
eurjchem-376	241	7	cm‐1	cm‐1	NOUN
eurjchem-376	241	8	characterized	characterize	VERB
eurjchem-376	241	9	for	for	ADP
eurjchem-376	241	10	amide	amide	PROPN
eurjchem-376	241	11	nh	nh	PROPN
eurjchem-376	241	12	.	.	PROPN
eurjchem-376	241	13	1h	1h	NUM
eurjchem-376	241	14	nmr	nmr	PROPN
eurjchem-376	241	15	spectrum	spectrum	NOUN
eurjchem-376	241	16	displayed	display	VERB
eurjchem-376	241	17	also	also	ADV
eurjchem-376	241	18	a	a	DET
eurjchem-376	241	19	triplet	triplet	NOUN
eurjchem-376	241	20	signal	signal	NOUN
eurjchem-376	241	21	at	at	ADP
eurjchem-376	241	22	1.3	1.3	NUM
eurjchem-376	241	23	ppm	ppm	NOUN
eurjchem-376	241	24	assigned	assign	VERB
eurjchem-376	241	25	for	for	ADP
eurjchem-376	241	26	ch3	ch3	PROPN
eurjchem-376	241	27	group	group	NOUN
eurjchem-376	241	28	,	,	PUNCT
eurjchem-376	241	29	a	a	DET
eurjchem-376	241	30	quartet	quartet	NOUN
eurjchem-376	241	31	signal	signal	NOUN
eurjchem-376	241	32	at	at	ADP
eurjchem-376	241	33	4.3	4.3	NUM
eurjchem-376	241	34	ppm	ppm	NOUN
eurjchem-376	241	35	due	due	ADP
eurjchem-376	241	36	to	to	ADP
eurjchem-376	241	37	ch2	ch2	VERB
eurjchem-376	241	38	and	and	CCONJ
eurjchem-376	241	39	signal	signal	VERB
eurjchem-376	241	40	at	at	ADP
eurjchem-376	241	41	8.8	8.8	NUM
eurjchem-376	241	42	ppm	ppm	NOUN
eurjchem-376	241	43	(	(	PUNCT
eurjchem-376	241	44	d2o	d2o	NOUN
eurjchem-376	241	45	exchangeable	exchangeable	ADJ
eurjchem-376	241	46	)	)	PUNCT
eurjchem-376	241	47	due	due	ADP
eurjchem-376	241	48	to	to	ADP
eurjchem-376	241	49	nh	nh	PROPN
eurjchem-376	241	50	proton	proton	NOUN
eurjchem-376	241	51	.	.	PUNCT
eurjchem-376	242	1	furthermore	furthermore	ADV
eurjchem-376	242	2	,	,	PUNCT
eurjchem-376	242	3	13c	13c	NOUN
eurjchem-376	242	4	nmr	nmr	NOUN
eurjchem-376	242	5	spectrum	spectrum	NOUN
eurjchem-376	242	6	of	of	ADP
eurjchem-376	242	7	compound	compound	NOUN
eurjchem-376	242	8	2	2	NUM
eurjchem-376	242	9	displayed	display	VERB
eurjchem-376	242	10	signals	signal	NOUN
eurjchem-376	242	11	at	at	ADP
eurjchem-376	242	12	172.2	172.2	NUM
eurjchem-376	242	13	and	and	CCONJ
eurjchem-376	242	14	175.4	175.4	NUM
eurjchem-376	242	15	corresponding	correspond	VERB
eurjchem-376	242	16	to	to	ADP
eurjchem-376	242	17	two	two	NUM
eurjchem-376	242	18	co	co	NOUN
eurjchem-376	242	19	respectively	respectively	ADV
eurjchem-376	242	20	.	.	PUNCT
eurjchem-376	243	1	the	the	DET
eurjchem-376	243	2	reactivity	reactivity	NOUN
eurjchem-376	243	3	of	of	ADP
eurjchem-376	243	4	the	the	DET
eurjchem-376	243	5	ester	ester	NOUN
eurjchem-376	243	6	2	2	NUM
eurjchem-376	243	7	towards	towards	ADP
eurjchem-376	243	8	some	some	DET
eurjchem-376	243	9	reagents	reagent	NOUN
eurjchem-376	243	10	with	with	ADP
eurjchem-376	243	11	the	the	DET
eurjchem-376	243	12	aim	aim	NOUN
eurjchem-376	243	13	of	of	ADP
eurjchem-376	243	14	the	the	DET
eurjchem-376	243	15	synthesis	synthesis	NOUN
eurjchem-376	243	16	of	of	ADP
eurjchem-376	243	17	novel	novel	NOUN
eurjchem-376	243	18	five	five	NUM
eurjchem-376	243	19	membered	membere	VERB
eurjchem-376	243	20	heterocycles	heterocycle	NOUN
eurjchem-376	243	21	was	be	AUX
eurjchem-376	243	22	investigated	investigate	VERB
eurjchem-376	243	23	.	.	PUNCT
eurjchem-376	244	1	thus	thus	ADV
eurjchem-376	244	2	,	,	PUNCT
eurjchem-376	244	3	the	the	DET
eurjchem-376	244	4	reaction	reaction	NOUN
eurjchem-376	244	5	of	of	ADP
eurjchem-376	244	6	compound	compound	NOUN
eurjchem-376	244	7	2	2	NUM
eurjchem-376	244	8	with	with	ADP
eurjchem-376	244	9	aromatic	aromatic	ADJ
eurjchem-376	244	10	aldehydes	aldehyde	NOUN
eurjchem-376	244	11	viz	viz	VERB
eurjchem-376	244	12	benzaldehyde	benzaldehyde	NOUN
eurjchem-376	244	13	afforded	afford	VERB
eurjchem-376	244	14	ethyl	ethyl	PROPN
eurjchem-376	244	15	2‐(6‐dibenzothiophen‐2‐yl‐	2‐(6‐dibenzothiophen‐2‐yl‐	PROPN
eurjchem-376	244	16	pyridazin‐3‐ylcarbamoyl)‐3‐phenylacrylate	pyridazin‐3‐ylcarbamoyl)‐3‐phenylacrylate	NOUN
eurjchem-376	244	17	(	(	PUNCT
eurjchem-376	244	18	3	3	NUM
eurjchem-376	244	19	)	)	PUNCT
eurjchem-376	244	20	.	.	PUNCT
eurjchem-376	245	1	cyclization	cyclization	NOUN
eurjchem-376	245	2	of	of	ADP
eurjchem-376	245	3	3	3	NUM
eurjchem-376	245	4	by	by	ADP
eurjchem-376	245	5	hydrazine	hydrazine	NOUN
eurjchem-376	245	6	hydrate	hydrate	NOUN
eurjchem-376	245	7	or	or	CCONJ
eurjchem-376	245	8	phenylhydrazine	phenylhydrazine	NOUN
eurjchem-376	245	9	to	to	PART
eurjchem-376	245	10	pyrazole	pyrazole	VERB
eurjchem-376	245	11	derivatives	derivative	NOUN
eurjchem-376	245	12	4a	4a	NOUN
eurjchem-376	245	13	,	,	PUNCT
eurjchem-376	245	14	b	b	PROPN
eurjchem-376	245	15	was	be	AUX
eurjchem-376	245	16	achieved	achieve	VERB
eurjchem-376	245	17	by	by	ADP
eurjchem-376	245	18	refluxing	refluxe	VERB
eurjchem-376	245	19	in	in	ADP
eurjchem-376	245	20	ethanol	ethanol	NOUN
eurjchem-376	245	21	.	.	PUNCT
eurjchem-376	246	1	the	the	DET
eurjchem-376	246	2	structures	structure	NOUN
eurjchem-376	246	3	of	of	ADP
eurjchem-376	246	4	the	the	DET
eurjchem-376	246	5	products	product	NOUN
eurjchem-376	246	6	were	be	AUX
eurjchem-376	246	7	assigned	assign	VERB
eurjchem-376	246	8	on	on	ADP
eurjchem-376	246	9	the	the	DET
eurjchem-376	246	10	basis	basis	NOUN
eurjchem-376	246	11	of	of	ADP
eurjchem-376	246	12	their	their	PRON
eurjchem-376	246	13	spectral	spectral	ADJ
eurjchem-376	246	14	data	datum	NOUN
eurjchem-376	246	15	and	and	CCONJ
eurjchem-376	246	16	elemental	elemental	ADJ
eurjchem-376	246	17	analysis	analysis	NOUN
eurjchem-376	246	18	.	.	PUNCT
eurjchem-376	247	1	on	on	ADP
eurjchem-376	247	2	the	the	DET
eurjchem-376	247	3	other	other	ADJ
eurjchem-376	247	4	hand	hand	NOUN
eurjchem-376	247	5	,	,	PUNCT
eurjchem-376	247	6	the	the	DET
eurjchem-376	247	7	reaction	reaction	NOUN
eurjchem-376	247	8	of	of	ADP
eurjchem-376	247	9	compound	compound	NOUN
eurjchem-376	247	10	2	2	NUM
eurjchem-376	247	11	with	with	ADP
eurjchem-376	247	12	salicyldehyde	salicyldehyde	PROPN
eurjchem-376	247	13	furnished	furnish	VERB
eurjchem-376	247	14	chromene	chromene	NOUN
eurjchem-376	247	15	derivative	derivative	ADJ
eurjchem-376	247	16	5	5	NUM
eurjchem-376	247	17	.	.	PUNCT
eurjchem-376	247	18	treatment	treatment	NOUN
eurjchem-376	247	19	of	of	ADP
eurjchem-376	247	20	compound	compound	NOUN
eurjchem-376	247	21	2	2	NUM
eurjchem-376	247	22	with	with	ADP
eurjchem-376	247	23	benzene	benzene	NOUN
eurjchem-376	247	24	diazonium	diazonium	NOUN
eurjchem-376	247	25	chloride	chloride	NOUN
eurjchem-376	247	26	afforded	afford	VERB
eurjchem-376	247	27	the	the	DET
eurjchem-376	247	28	hydrazone	hydrazone	NOUN
eurjchem-376	247	29	derivative	derivative	NOUN
eurjchem-376	247	30	6	6	NUM
eurjchem-376	247	31	,	,	PUNCT
eurjchem-376	247	32	which	which	PRON
eurjchem-376	247	33	in	in	ADP
eurjchem-376	247	34	turn	turn	NOUN
eurjchem-376	247	35	reacted	react	VERB
eurjchem-376	247	36	with	with	ADP
eurjchem-376	247	37	hydrazine	hydrazine	NOUN
eurjchem-376	247	38	hydrate	hydrate	NOUN
eurjchem-376	247	39	to	to	PART
eurjchem-376	247	40	give	give	VERB
eurjchem-376	247	41	1,2,3‐	1,2,3‐	NUM
eurjchem-376	247	42	triazole	triazole	NOUN
eurjchem-376	247	43	derivative	derivative	ADJ
eurjchem-376	247	44	7	7	NUM
eurjchem-376	247	45	(	(	PUNCT
eurjchem-376	247	46	scheme	scheme	NOUN
eurjchem-376	247	47	2	2	NUM
eurjchem-376	247	48	)	)	PUNCT
eurjchem-376	247	49	.	.	PUNCT
eurjchem-376	248	1	on	on	ADP
eurjchem-376	248	2	the	the	DET
eurjchem-376	248	3	other	other	ADJ
eurjchem-376	248	4	hand	hand	NOUN
eurjchem-376	248	5	,	,	PUNCT
eurjchem-376	248	6	the	the	DET
eurjchem-376	248	7	reaction	reaction	NOUN
eurjchem-376	248	8	of	of	ADP
eurjchem-376	248	9	compound	compound	NOUN
eurjchem-376	248	10	2	2	NUM
eurjchem-376	248	11	with	with	ADP
eurjchem-376	248	12	phenyl	phenyl	NOUN
eurjchem-376	248	13	isothiocyanate	isothiocyanate	NOUN
eurjchem-376	248	14	8	8	NUM
eurjchem-376	248	15	in	in	ADP
eurjchem-376	248	16	dimethylformamide	dimethylformamide	NOUN
eurjchem-376	248	17	solution	solution	NOUN
eurjchem-376	248	18	afforded	afford	VERB
eurjchem-376	248	19	the	the	DET
eurjchem-376	248	20	intermediate	intermediate	ADJ
eurjchem-376	248	21	9	9	NUM
eurjchem-376	248	22	.	.	NOUN
eurjchem-376	248	23	cyclization	cyclization	NOUN
eurjchem-376	248	24	of	of	ADP
eurjchem-376	248	25	the	the	DET
eurjchem-376	248	26	latter	latter	ADJ
eurjchem-376	248	27	by	by	ADP
eurjchem-376	248	28	chloroacetone	chloroacetone	PROPN
eurjchem-376	248	29	gave	give	VERB
eurjchem-376	248	30	thiophene	thiophene	NOUN
eurjchem-376	248	31	derivative	derivative	ADJ
eurjchem-376	248	32	10	10	NUM
eurjchem-376	248	33	(	(	PUNCT
eurjchem-376	248	34	scheme	scheme	NOUN
eurjchem-376	248	35	3	3	NUM
eurjchem-376	248	36	)	)	PUNCT
eurjchem-376	248	37	.	.	PUNCT
eurjchem-376	249	1	also	also	ADV
eurjchem-376	249	2	,	,	PUNCT
eurjchem-376	249	3	the	the	DET
eurjchem-376	249	4	reactivity	reactivity	NOUN
eurjchem-376	249	5	of	of	ADP
eurjchem-376	249	6	ester	ester	NOUN
eurjchem-376	249	7	2	2	NUM
eurjchem-376	249	8	for	for	ADP
eurjchem-376	249	9	the	the	DET
eurjchem-376	249	10	synthesis	synthesis	NOUN
eurjchem-376	249	11	of	of	ADP
eurjchem-376	249	12	six	six	NUM
eurjchem-376	249	13	membered	membere	VERB
eurjchem-376	249	14	heterocycles	heterocycle	NOUN
eurjchem-376	249	15	was	be	AUX
eurjchem-376	249	16	depicted	depict	VERB
eurjchem-376	249	17	.	.	PUNCT
eurjchem-376	250	1	thus	thus	ADV
eurjchem-376	250	2	,	,	PUNCT
eurjchem-376	250	3	the	the	DET
eurjchem-376	250	4	reaction	reaction	NOUN
eurjchem-376	250	5	of	of	ADP
eurjchem-376	250	6	ester	ester	NOUN
eurjchem-376	250	7	2	2	NUM
eurjchem-376	250	8	with	with	ADP
eurjchem-376	250	9	urea	urea	NOUN
eurjchem-376	250	10	and/or	and/or	CCONJ
eurjchem-376	250	11	thiourea	thiourea	NOUN
eurjchem-376	250	12	in	in	ADP
eurjchem-376	250	13	ethanolic	ethanolic	ADJ
eurjchem-376	250	14	sodium	sodium	NOUN
eurjchem-376	250	15	ethoxide	ethoxide	NOUN
eurjchem-376	250	16	solution	solution	NOUN
eurjchem-376	250	17	afforded	afford	VERB
eurjchem-376	250	18	pyrimidinones	pyrimidinone	NOUN
eurjchem-376	250	19	11a	11a	NUM
eurjchem-376	250	20	,	,	PUNCT
eurjchem-376	250	21	b.	b.	PROPN
eurjchem-376	250	22	behalo	behalo	NOUN
eurjchem-376	250	23	and	and	CCONJ
eurjchem-376	250	24	aly	aly	PROPN
eurjchem-376	250	25	/	/	SYM
eurjchem-376	250	26	european	european	PROPN
eurjchem-376	250	27	journal	journal	PROPN
eurjchem-376	250	28	of	of	ADP
eurjchem-376	250	29	chemistry	chemistry	NOUN
eurjchem-376	250	30	2	2	NUM
eurjchem-376	250	31	(	(	PUNCT
eurjchem-376	250	32	3	3	NUM
eurjchem-376	250	33	)	)	PUNCT
eurjchem-376	250	34	(	(	PUNCT
eurjchem-376	250	35	2011	2011	NUM
eurjchem-376	250	36	)	)	PUNCT
eurjchem-376	250	37	295‐299	295‐299	NOUN
eurjchem-376	250	38	299	299	NUM
eurjchem-376	250	39	scheme	scheme	NOUN
eurjchem-376	250	40	5	5	NUM
eurjchem-376	250	41	ir	ir	PROPN
eurjchem-376	250	42	spectra	spectra	PROPN
eurjchem-376	250	43	displayed	display	VERB
eurjchem-376	250	44	absorption	absorption	NOUN
eurjchem-376	250	45	band	band	NOUN
eurjchem-376	250	46	at	at	ADP
eurjchem-376	250	47	3375‐3250	3375‐3250	NUM
eurjchem-376	250	48	cm‐1	cm‐1	NOUN
eurjchem-376	250	49	corresponding	correspond	VERB
eurjchem-376	250	50	to	to	ADP
eurjchem-376	250	51	nh	nh	PROPN
eurjchem-376	250	52	group	group	NOUN
eurjchem-376	250	53	.	.	PUNCT
eurjchem-376	251	1	treatment	treatment	NOUN
eurjchem-376	251	2	of	of	ADP
eurjchem-376	251	3	pyrimidinones	pyrimidinone	NOUN
eurjchem-376	251	4	11a	11a	NUM
eurjchem-376	251	5	,	,	PUNCT
eurjchem-376	251	6	b	b	NOUN
eurjchem-376	251	7	with	with	ADP
eurjchem-376	251	8	aryl	aryl	NOUN
eurjchem-376	251	9	diazonium	diazonium	NOUN
eurjchem-376	251	10	chloride	chloride	NOUN
eurjchem-376	251	11	or	or	CCONJ
eurjchem-376	251	12	aromatic	aromatic	ADJ
eurjchem-376	251	13	aldehydes	aldehyde	NOUN
eurjchem-376	251	14	result	result	VERB
eurjchem-376	251	15	in	in	ADP
eurjchem-376	251	16	the	the	DET
eurjchem-376	251	17	formation	formation	NOUN
eurjchem-376	251	18	of	of	ADP
eurjchem-376	251	19	pyrimidinone	pyrimidinone	ADJ
eurjchem-376	251	20	12a‐d	12a‐d	NOUN
eurjchem-376	251	21	and	and	CCONJ
eurjchem-376	251	22	13a‐d	13a‐d	NOUN
eurjchem-376	251	23	,	,	PUNCT
eurjchem-376	251	24	respectively	respectively	ADV
eurjchem-376	251	25	(	(	PUNCT
eurjchem-376	251	26	scheme	scheme	NOUN
eurjchem-376	251	27	4	4	NUM
eurjchem-376	251	28	)	)	PUNCT
eurjchem-376	251	29	.	.	PUNCT
eurjchem-376	252	1	the	the	DET
eurjchem-376	252	2	reaction	reaction	NOUN
eurjchem-376	252	3	of	of	ADP
eurjchem-376	252	4	compound	compound	NOUN
eurjchem-376	252	5	2	2	NUM
eurjchem-376	252	6	with	with	ADP
eurjchem-376	252	7	active	active	ADJ
eurjchem-376	252	8	methylene	methylene	NOUN
eurjchem-376	252	9	reagents	reagent	NOUN
eurjchem-376	252	10	viz	viz	ADP
eurjchem-376	252	11	malononitrile	malononitrile	NOUN
eurjchem-376	252	12	and	and	CCONJ
eurjchem-376	252	13	ethyl	ethyl	PROPN
eurjchem-376	252	14	cyanoacetate	cyanoacetate	NOUN
eurjchem-376	252	15	in	in	ADP
eurjchem-376	252	16	dimethylformamide	dimethylformamide	NOUN
eurjchem-376	252	17	containing	contain	VERB
eurjchem-376	252	18	triethyl	triethyl	NOUN
eurjchem-376	252	19	amine	amine	NOUN
eurjchem-376	252	20	afforded	afford	VERB
eurjchem-376	252	21	pyridinone	pyridinone	NOUN
eurjchem-376	252	22	derivatives	derivative	NOUN
eurjchem-376	252	23	14a	14a	NOUN
eurjchem-376	252	24	,	,	PUNCT
eurjchem-376	252	25	b	b	NOUN
eurjchem-376	252	26	,	,	PUNCT
eurjchem-376	252	27	respectively	respectively	ADV
eurjchem-376	252	28	(	(	PUNCT
eurjchem-376	252	29	scheme	scheme	NOUN
eurjchem-376	252	30	5	5	NUM
eurjchem-376	252	31	)	)	PUNCT
eurjchem-376	252	32	.	.	PUNCT
eurjchem-376	253	1	similarly	similarly	ADV
eurjchem-376	253	2	,	,	PUNCT
eurjchem-376	253	3	the	the	DET
eurjchem-376	253	4	reaction	reaction	NOUN
eurjchem-376	253	5	of	of	ADP
eurjchem-376	253	6	2	2	NUM
eurjchem-376	253	7	with	with	ADP
eurjchem-376	253	8	α‐cyanocinnamonitrile	α‐cyanocinnamonitrile	NUM
eurjchem-376	253	9	furnished	furnish	VERB
eurjchem-376	253	10	ethyl	ethyl	PROPN
eurjchem-376	253	11	6‐amino‐5‐cyano‐1‐(6‐dibenzothiophen‐2‐yl‐	6‐amino‐5‐cyano‐1‐(6‐dibenzothiophen‐2‐yl‐	NUM
eurjchem-376	253	12	pyridazin‐3‐yl)‐2‐oxo‐4‐phenyl‐1,2‐dihydropyridine‐3‐	pyridazin‐3‐yl)‐2‐oxo‐4‐phenyl‐1,2‐dihydropyridine‐3‐	NOUN
eurjchem-376	253	13	carboxylate	carboxylate	NOUN
eurjchem-376	253	14	(	(	PUNCT
eurjchem-376	253	15	15	15	NUM
eurjchem-376	253	16	)	)	PUNCT
eurjchem-376	253	17	.	.	PUNCT
eurjchem-376	254	1	4	4	X
eurjchem-376	254	2	.	.	X
eurjchem-376	254	3	conclusion	conclusion	NOUN
eurjchem-376	254	4	in	in	ADP
eurjchem-376	254	5	the	the	DET
eurjchem-376	254	6	present	present	ADJ
eurjchem-376	254	7	paper	paper	NOUN
eurjchem-376	254	8	we	we	PRON
eurjchem-376	254	9	describe	describe	VERB
eurjchem-376	254	10	the	the	DET
eurjchem-376	254	11	reaction	reaction	NOUN
eurjchem-376	254	12	of	of	ADP
eurjchem-376	254	13	ethyl	ethyl	PROPN
eurjchem-376	254	14	3‐(6‐	3‐(6‐	NOUN
eurjchem-376	255	1	dibenzothiophen‐2‐yl‐pyridazin‐3‐ylamino)‐3‐oxopropanoate	dibenzothiophen‐2‐yl‐pyridazin‐3‐ylamino)‐3‐oxopropanoate	NOUN
eurjchem-376	255	2	with	with	ADP
eurjchem-376	255	3	various	various	ADJ
eurjchem-376	255	4	reagents	reagent	NOUN
eurjchem-376	255	5	providing	provide	VERB
eurjchem-376	255	6	novel	novel	NOUN
eurjchem-376	255	7	five	five	NUM
eurjchem-376	255	8	and	and	CCONJ
eurjchem-376	255	9	six	six	NUM
eurjchem-376	255	10	membered	membere	VERB
eurjchem-376	255	11	heterocycle	heterocycle	NOUN
eurjchem-376	255	12	derivatives	derivative	NOUN
eurjchem-376	255	13	attached	attach	VERB
eurjchem-376	255	14	to	to	ADP
eurjchem-376	255	15	pyridazine	pyridazine	NOUN
eurjchem-376	255	16	and	and	CCONJ
eurjchem-376	255	17	dibenzothiophene	dibenzothiophene	ADJ
eurjchem-376	255	18	moieties	moiety	NOUN
eurjchem-376	255	19	.	.	PUNCT
eurjchem-376	256	1	the	the	DET
eurjchem-376	256	2	structures	structure	NOUN
eurjchem-376	256	3	of	of	ADP
eurjchem-376	256	4	all	all	DET
eurjchem-376	256	5	products	product	NOUN
eurjchem-376	256	6	were	be	AUX
eurjchem-376	256	7	confirmed	confirm	VERB
eurjchem-376	256	8	by	by	ADP
eurjchem-376	256	9	the	the	DET
eurjchem-376	256	10	elemental	elemental	ADJ
eurjchem-376	256	11	analysis	analysis	NOUN
eurjchem-376	256	12	and	and	CCONJ
eurjchem-376	256	13	spectroscopic	spectroscopic	ADJ
eurjchem-376	256	14	studies	study	NOUN
eurjchem-376	256	15	.	.	PUNCT
eurjchem-376	257	1	references	reference	NOUN
eurjchem-376	257	2	[	[	X
eurjchem-376	257	3	1	1	NUM
eurjchem-376	257	4	]	]	PUNCT
eurjchem-376	257	5	.	.	PUNCT
eurjchem-376	258	1	butnariu	butnariu	PROPN
eurjchem-376	258	2	,	,	PUNCT
eurjchem-376	258	3	r.	r.	PROPN
eurjchem-376	258	4	m.	m.	PROPN
eurjchem-376	258	5	;	;	PUNCT
eurjchem-376	258	6	mangalagiu	mangalagiu	PROPN
eurjchem-376	258	7	,	,	PUNCT
eurjchem-376	258	8	i.	i.	PROPN
eurjchem-376	258	9	i.	i.	PROPN
eurjchem-376	258	10	bioorg	bioorg	PROPN
eurjchem-376	258	11	.	.	PUNCT
eurjchem-376	259	1	med	med	PROPN
eurjchem-376	259	2	.	.	PUNCT
eurjchem-376	259	3	chem	chem	PROPN
eurjchem-376	259	4	.	.	PUNCT
eurjchem-376	260	1	2009	2009	NUM
eurjchem-376	260	2	,	,	PUNCT
eurjchem-376	260	3	17(7	17(7	NUM
eurjchem-376	260	4	)	)	PUNCT
eurjchem-376	260	5	,	,	PUNCT
eurjchem-376	260	6	2823‐	2823‐	NUM
eurjchem-376	260	7	2829	2829	NUM
eurjchem-376	260	8	.	.	PUNCT
eurjchem-376	261	1	[	[	X
eurjchem-376	261	2	2	2	NUM
eurjchem-376	261	3	]	]	PUNCT
eurjchem-376	261	4	.	.	PUNCT
eurjchem-376	262	1	grey	grey	PROPN
eurjchem-376	262	2	,	,	PUNCT
eurjchem-376	262	3	r.	r.	PROPN
eurjchem-376	262	4	;	;	PUNCT
eurjchem-376	262	5	pierce	pierce	PROPN
eurjchem-376	262	6	,	,	PUNCT
eurjchem-376	262	7	a.	a.	PROPN
eurjchem-376	262	8	c.	c.	PROPN
eurjchem-376	262	9	;	;	PUNCT
eurjchem-376	262	10	bemis	bemis	PROPN
eurjchem-376	262	11	,	,	PUNCT
eurjchem-376	262	12	g.	g.	PROPN
eurjchem-376	262	13	w.	w.	PROPN
eurjchem-376	262	14	;	;	PUNCT
eurjchem-376	262	15	jacobs	jacobs	PROPN
eurjchem-376	262	16	,	,	PUNCT
eurjchem-376	262	17	m.	m.	PROPN
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eurjchem-376	262	26	,	,	PUNCT
eurjchem-376	262	27	r.	r.	PROPN
eurjchem-376	262	28	;	;	PUNCT
eurjchem-376	262	29	mohal	mohal	NOUN
eurjchem-376	262	30	,	,	PUNCT
eurjchem-376	262	31	n.	n.	NOUN
eurjchem-376	262	32	;	;	PUNCT
eurjchem-376	262	33	green	green	PROPN
eurjchem-376	262	34	,	,	PUNCT
eurjchem-376	262	35	j.	j.	PROPN
eurjchem-376	262	36	bioorg	bioorg	PROPN
eurjchem-376	262	37	.	.	PUNCT
eurjchem-376	263	1	med	med	PROPN
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eurjchem-376	264	2	.	.	PUNCT
eurjchem-376	265	1	2009	2009	NUM
eurjchem-376	265	2	,	,	PUNCT
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eurjchem-376	265	4	)	)	PUNCT
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eurjchem-376	266	1	[	[	X
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eurjchem-376	298	21	,	,	PUNCT
eurjchem-376	298	22	p.	p.	NOUN
eurjchem-376	298	23	;	;	PUNCT
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eurjchem-376	298	25	,	,	PUNCT
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eurjchem-376	300	2	,	,	PUNCT
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eurjchem-376	300	4	,	,	PUNCT
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eurjchem-376	300	6	.	.	PUNCT
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eurjchem-376	301	3	]	]	PUNCT
eurjchem-376	301	4	.	.	PUNCT
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eurjchem-376	301	23	,	,	PUNCT
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eurjchem-376	301	25	,	,	PUNCT
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eurjchem-376	301	27	.	.	PUNCT
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eurjchem-376	302	3	]	]	PUNCT
eurjchem-376	302	4	.	.	PUNCT
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eurjchem-376	303	2	,	,	PUNCT
eurjchem-376	303	3	m.	m.	PROPN
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eurjchem-376	303	5	;	;	PUNCT
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eurjchem-376	303	7	,	,	PUNCT
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eurjchem-376	303	10	;	;	PUNCT
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eurjchem-376	303	17	m.	m.	PROPN
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eurjchem-376	303	23	;	;	PUNCT
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eurjchem-376	303	25	,	,	PUNCT
eurjchem-376	303	26	c.	c.	PROPN
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eurjchem-376	303	31	j.	j.	PROPN
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eurjchem-376	303	33	.	.	PUNCT
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eurjchem-376	304	2	.	.	PUNCT
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eurjchem-376	305	2	,	,	PUNCT
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eurjchem-376	305	4	)	)	PUNCT
eurjchem-376	305	5	,	,	PUNCT
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eurjchem-376	305	7	.	.	PUNCT
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eurjchem-376	306	3	]	]	PUNCT
eurjchem-376	306	4	.	.	PUNCT
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eurjchem-376	307	13	;	;	PUNCT
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eurjchem-376	307	17	;	;	PUNCT
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eurjchem-376	307	19	,	,	PUNCT
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eurjchem-376	308	5	.	.	PUNCT
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eurjchem-376	309	2	,	,	PUNCT
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eurjchem-376	309	4	)	)	PUNCT
eurjchem-376	309	5	,	,	PUNCT
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eurjchem-376	309	7	.	.	PUNCT
eurjchem-376	310	1	[	[	X
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eurjchem-376	310	3	]	]	PUNCT
eurjchem-376	310	4	.	.	PUNCT
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eurjchem-376	311	2	,	,	PUNCT
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eurjchem-376	311	13	eur	eur	PROPN
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eurjchem-376	312	5	.	.	PUNCT
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eurjchem-376	313	2	,	,	PUNCT
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eurjchem-376	313	4	,	,	PUNCT
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eurjchem-376	313	6	.	.	PUNCT
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eurjchem-376	314	3	]	]	PUNCT
eurjchem-376	314	4	.	.	PUNCT
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eurjchem-376	315	2	,	,	PUNCT
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eurjchem-376	315	4	;	;	PUNCT
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eurjchem-376	315	6	,	,	PUNCT
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eurjchem-376	315	8	;	;	PUNCT
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eurjchem-376	315	12	m.	m.	PROPN
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eurjchem-376	315	17	,	,	PUNCT
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eurjchem-376	316	3	]	]	PUNCT
eurjchem-376	316	4	.	.	PUNCT
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eurjchem-376	317	4	;	;	PUNCT
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eurjchem-376	317	6	,	,	PUNCT
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eurjchem-376	318	2	.	.	PUNCT
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eurjchem-376	319	2	,	,	PUNCT
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eurjchem-376	319	4	,	,	PUNCT
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eurjchem-376	319	6	.	.	PUNCT
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eurjchem-376	320	3	]	]	PUNCT
eurjchem-376	320	4	.	.	PUNCT
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eurjchem-376	323	2	.	.	PUNCT
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eurjchem-376	324	2	,	,	PUNCT
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eurjchem-376	325	4	.	.	PUNCT
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eurjchem-376	328	2	,	,	PUNCT
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eurjchem-376	332	2	,	,	PUNCT
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eurjchem-376	333	31	behalo	behalo	NOUN
eurjchem-376	333	32	,	,	PUNCT
eurjchem-376	333	33	m.	m.	NOUN
eurjchem-376	333	34	s.	s.	PROPN
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eurjchem-376	334	2	.	.	PUNCT
eurjchem-376	335	1	2009	2009	NUM
eurjchem-376	335	2	,	,	PUNCT
eurjchem-376	335	3	11(11	11(11	NUM
eurjchem-376	335	4	)	)	PUNCT
eurjchem-376	335	5	,	,	PUNCT
eurjchem-376	335	6	2265‐2268	2265‐2268	NUM
eurjchem-376	335	7	.	.	PUNCT
eurjchem-376	336	1	[	[	X
eurjchem-376	336	2	22	22	NUM
eurjchem-376	336	3	]	]	PUNCT
eurjchem-376	336	4	.	.	PUNCT
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eurjchem-376	337	2	,	,	PUNCT
eurjchem-376	337	3	y.	y.	PROPN
eurjchem-376	337	4	a.	a.	PROPN
eurjchem-376	337	5	;	;	PUNCT
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eurjchem-376	337	7	,	,	PUNCT
eurjchem-376	337	8	i.	i.	PROPN
eurjchem-376	337	9	g.	g.	PROPN
eurjchem-376	337	10	;	;	PUNCT
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eurjchem-376	337	12	,	,	PUNCT
eurjchem-376	337	13	s.	s.	PROPN
eurjchem-376	337	14	g.	g.	PROPN
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eurjchem-376	337	17	,	,	PUNCT
eurjchem-376	337	18	m.	m.	NOUN
eurjchem-376	337	19	s.	s.	PROPN
eurjchem-376	337	20	sulf	sulf	PROPN
eurjchem-376	337	21	.	.	PUNCT
eurjchem-376	338	1	lett	lett	PROPN
eurjchem-376	338	2	.	.	PUNCT
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eurjchem-376	339	2	,	,	PUNCT
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eurjchem-376	339	4	)	)	PUNCT
eurjchem-376	339	5	,	,	PUNCT
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eurjchem-376	339	7	.	.	PUNCT
eurjchem-376	340	1	[	[	X
eurjchem-376	340	2	23	23	NUM
eurjchem-376	340	3	]	]	PUNCT
eurjchem-376	340	4	.	.	PUNCT
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eurjchem-376	341	2	,	,	PUNCT
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eurjchem-376	341	4	a.	a.	PROPN
eurjchem-376	341	5	;	;	PUNCT
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eurjchem-376	341	7	,	,	PUNCT
eurjchem-376	341	8	i.	i.	PROPN
eurjchem-376	341	9	g.	g.	PROPN
eurjchem-376	341	10	;	;	PUNCT
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eurjchem-376	341	18	a.	a.	NOUN
eurjchem-376	341	19	a.	a.	PROPN
eurjchem-376	341	20	;	;	PUNCT
eurjchem-376	341	21	donia	donia	PROPN
eurjchem-376	341	22	,	,	PUNCT
eurjchem-376	341	23	s.	s.	PROPN
eurjchem-376	341	24	g.	g.	PROPN
eurjchem-376	341	25	olaj	olaj	PROPN
eurjchem-376	341	26	,	,	PUNCT
eurjchem-376	341	27	szappan	szappan	NOUN
eurjchem-376	341	28	,	,	PUNCT
eurjchem-376	341	29	kozmetika	kozmetika	PROPN
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eurjchem-376	341	31	,	,	PUNCT
eurjchem-376	341	32	57(4	57(4	NUM
eurjchem-376	341	33	)	)	PUNCT
eurjchem-376	341	34	,	,	PUNCT
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eurjchem-376	341	36	.	.	PUNCT
eurjchem-376	342	1	[	[	X
eurjchem-376	342	2	24	24	NUM
eurjchem-376	342	3	]	]	PUNCT
eurjchem-376	342	4	.	.	PUNCT
eurjchem-376	343	1	behalo	behalo	PROPN
eurjchem-376	343	2	,	,	PUNCT
eurjchem-376	343	3	m.	m.	NOUN
eurjchem-376	343	4	s.	s.	PROPN
eurjchem-376	343	5	phosphorus	phosphorus	PROPN
eurjchem-376	343	6	,	,	PUNCT
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eurjchem-376	343	8	and	and	CCONJ
eurjchem-376	343	9	silicon	silicon	NOUN
eurjchem-376	343	10	and	and	CCONJ
eurjchem-376	343	11	the	the	DET
eurjchem-376	343	12	relat	relat	NOUN
eurjchem-376	343	13	.	.	PUNCT
eurjchem-376	344	1	elements	element	NOUN
eurjchem-376	344	2	,	,	PUNCT
eurjchem-376	344	3	2009	2009	NUM
eurjchem-376	344	4	,	,	PUNCT
eurjchem-376	344	5	184(1	184(1	NUM
eurjchem-376	344	6	)	)	PUNCT
eurjchem-376	344	7	,	,	PUNCT
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eurjchem-376	344	9	.	.	PUNCT
eurjchem-376	345	1	[	[	X
eurjchem-376	345	2	25	25	NUM
eurjchem-376	345	3	]	]	PUNCT
eurjchem-376	345	4	.	.	PUNCT
eurjchem-376	346	1	donia	donia	PROPN
eurjchem-376	346	2	,	,	PUNCT
eurjchem-376	346	3	s.	s.	PROPN
eurjchem-376	346	4	g.	g.	PROPN
eurjchem-376	346	5	;	;	PUNCT
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eurjchem-376	346	7	s.	s.	PROPN
eurjchem-376	346	8	a.	a.	PROPN
eurjchem-376	346	9	;	;	PUNCT
eurjchem-376	346	10	el‐sawy	el‐sawy	PROPN
eurjchem-376	346	11	,	,	PUNCT
eurjchem-376	346	12	a.	a.	NOUN
eurjchem-376	346	13	a.	a.	NOUN
eurjchem-376	346	14	;	;	PUNCT
eurjchem-376	346	15	farouk	farouk	PROPN
eurjchem-376	346	16	,	,	PUNCT
eurjchem-376	346	17	a.	a.	PROPN
eurjchem-376	346	18	a.	a.	PROPN
eurjchem-376	346	19	j.	j.	PROPN
eurjchem-376	346	20	serb	serb	PROPN
eurjchem-376	346	21	.	.	PUNCT
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eurjchem-376	347	2	.	.	PUNCT
eurjchem-376	348	1	soc	soc	PROPN
eurjchem-376	348	2	.	.	PUNCT
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eurjchem-376	349	2	,	,	PUNCT
eurjchem-376	349	3	53	53	NUM
eurjchem-376	349	4	,	,	PUNCT
eurjchem-376	349	5	543‐550	543‐550	NUM
eurjchem-376	349	6	.	.	PUNCT