id	sid	tid	token	lemma	pos
eurjchem-479	1	1	untitled	untitle	VERB
eurjchem-479	1	2	european	european	PROPN
eurjchem-479	1	3	journal	journal	PROPN
eurjchem-479	1	4	of	of	ADP
eurjchem-479	1	5	chemistry	chemistry	NOUN
eurjchem-479	1	6	2	2	NUM
eurjchem-479	1	7	(	(	PUNCT
eurjchem-479	1	8	4	4	NUM
eurjchem-479	1	9	)	)	PUNCT
eurjchem-479	1	10	(	(	PUNCT
eurjchem-479	1	11	2011	2011	NUM
eurjchem-479	1	12	)	)	PUNCT
eurjchem-479	1	13	514‐518	514‐518	PROPN
eurjchem-479	1	14	european	european	PROPN
eurjchem-479	1	15	journal	journal	PROPN
eurjchem-479	1	16	of	of	ADP
eurjchem-479	1	17	chemistry	chemistry	NOUN
eurjchem-479	1	18	issn	issn	PROPN
eurjchem-479	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-479	1	20	(	(	PUNCT
eurjchem-479	1	21	print	print	NOUN
eurjchem-479	1	22	)	)	PUNCT
eurjchem-479	1	23	/	/	SYM
eurjchem-479	1	24	issn	issn	PROPN
eurjchem-479	1	25	2153‐2257	2153‐2257	NUM
eurjchem-479	1	26	(	(	PUNCT
eurjchem-479	1	27	online	online	ADJ
eurjchem-479	1	28	)	)	PUNCT
eurjchem-479	1	29			NOUN
eurjchem-479	1	30	2011	2011	NUM
eurjchem-479	1	31	eurjchem	eurjchem	PROPN
eurjchem-479	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-479	1	33	/	/	SYM
eurjchem-479	1	34	eurjchem.2.4.514‐518.479	eurjchem.2.4.514‐518.479	ADJ
eurjchem-479	1	35	european	european	ADJ
eurjchem-479	1	36	journal	journal	PROPN
eurjchem-479	1	37	of	of	ADP
eurjchem-479	1	38	chemistry	chemistry	PROPN
eurjchem-479	1	39	journal	journal	PROPN
eurjchem-479	1	40	homepage	homepage	NOUN
eurjchem-479	1	41	:	:	PUNCT
eurjchem-479	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-479	1	43	synthesis	synthesis	NOUN
eurjchem-479	1	44	and	and	CCONJ
eurjchem-479	1	45	reactions	reaction	NOUN
eurjchem-479	1	46	of	of	ADP
eurjchem-479	1	47	3‐aminotetrachloroquinazolin‐2,4‐dione	3‐aminotetrachloroquinazolin‐2,4‐dione	NUM
eurjchem-479	1	48	mamdouh	mamdouh	NOUN
eurjchem-479	1	49	adly	adly	PROPN
eurjchem-479	1	50	hassan	hassan	PROPN
eurjchem-479	1	51	,	,	PUNCT
eurjchem-479	1	52	ahmed	ahmed	PROPN
eurjchem-479	1	53	mohamed	mohamed	PROPN
eurjchem-479	1	54	mosalem	mosalem	PROPN
eurjchem-479	1	55	younes	younes	PROPN
eurjchem-479	1	56	,	,	PUNCT
eurjchem-479	1	57	mohamed	mohamed	PROPN
eurjchem-479	1	58	mobark	mobark	PROPN
eurjchem-479	1	59	taha	taha	PROPN
eurjchem-479	1	60	and	and	CCONJ
eurjchem-479	1	61	abou‐bakr	abou‐bakr	ADJ
eurjchem-479	1	62	haredy	haredy	NOUN
eurjchem-479	1	63	abdel‐monsef	abdel‐monsef	PROPN
eurjchem-479	1	64	*	*	SYM
eurjchem-479	1	65	chemistry	chemistry	NOUN
eurjchem-479	1	66	department	department	NOUN
eurjchem-479	1	67	,	,	PUNCT
eurjchem-479	1	68	faculty	faculty	NOUN
eurjchem-479	1	69	of	of	ADP
eurjchem-479	1	70	science	science	NOUN
eurjchem-479	1	71	,	,	PUNCT
eurjchem-479	1	72	south	south	PROPN
eurjchem-479	1	73	valley	valley	PROPN
eurjchem-479	1	74	university	university	PROPN
eurjchem-479	1	75	,	,	PUNCT
eurjchem-479	1	76	qena‐83523	qena‐83523	PROPN
eurjchem-479	1	77	,	,	PUNCT
eurjchem-479	1	78	egypt	egypt	PROPN
eurjchem-479	1	79	*	*	PUNCT
eurjchem-479	1	80	corresponding	correspond	VERB
eurjchem-479	1	81	author	author	NOUN
eurjchem-479	1	82	at	at	ADP
eurjchem-479	1	83	:	:	PUNCT
eurjchem-479	1	84	chemistry	chemistry	NOUN
eurjchem-479	1	85	department	department	NOUN
eurjchem-479	1	86	,	,	PUNCT
eurjchem-479	1	87	faculty	faculty	NOUN
eurjchem-479	1	88	of	of	ADP
eurjchem-479	1	89	science	science	NOUN
eurjchem-479	1	90	,	,	PUNCT
eurjchem-479	1	91	south	south	PROPN
eurjchem-479	1	92	valley	valley	PROPN
eurjchem-479	1	93	university	university	PROPN
eurjchem-479	1	94	,	,	PUNCT
eurjchem-479	1	95	qena‐83523	qena‐83523	PROPN
eurjchem-479	1	96	,	,	PUNCT
eurjchem-479	1	97	egypt	egypt	PROPN
eurjchem-479	1	98	.	.	PUNCT
eurjchem-479	2	1	tel	tel	PROPN
eurjchem-479	2	2	.	.	PUNCT
eurjchem-479	2	3	:	:	PUNCT
eurjchem-479	3	1	+20.96.5211281	+20.96.5211281	NUM
eurjchem-479	3	2	;	;	PUNCT
eurjchem-479	3	3	fax	fax	NOUN
eurjchem-479	3	4	:	:	PUNCT
eurjchem-479	3	5	+20.96.5211279	+20.96.5211279	NUM
eurjchem-479	3	6	.	.	PUNCT
eurjchem-479	3	7	e‐mail	e‐mail	PUNCT
eurjchem-479	4	1	address	address	NOUN
eurjchem-479	4	2	:	:	PUNCT
eurjchem-479	4	3	bakooos2004@yahoo.com	bakooos2004@yahoo.com	X
eurjchem-479	4	4	(	(	PUNCT
eurjchem-479	4	5	a.h	a.h	PROPN
eurjchem-479	4	6	.	.	PROPN
eurjchem-479	4	7	abdel‐monsef	abdel‐monsef	PROPN
eurjchem-479	4	8	)	)	PUNCT
eurjchem-479	4	9	.	.	PUNCT
eurjchem-479	5	1	article	article	NOUN
eurjchem-479	5	2	information	information	PROPN
eurjchem-479	5	3	abstract	abstract	ADV
eurjchem-479	5	4	received	receive	VERB
eurjchem-479	5	5	:	:	PUNCT
eurjchem-479	5	6	21	21	NUM
eurjchem-479	5	7	june	june	PROPN
eurjchem-479	5	8	2011	2011	NUM
eurjchem-479	5	9	received	receive	VERB
eurjchem-479	5	10	in	in	ADP
eurjchem-479	5	11	revised	revise	VERB
eurjchem-479	5	12	form	form	NOUN
eurjchem-479	5	13	:	:	PUNCT
eurjchem-479	5	14	31	31	NUM
eurjchem-479	5	15	july	july	PROPN
eurjchem-479	5	16	2011	2011	NUM
eurjchem-479	5	17	accepted	accept	VERB
eurjchem-479	5	18	:	:	PUNCT
eurjchem-479	5	19	31	31	NUM
eurjchem-479	5	20	july	july	PROPN
eurjchem-479	5	21	2011	2011	NUM
eurjchem-479	5	22	online	online	ADV
eurjchem-479	5	23	:	:	PUNCT
eurjchem-479	5	24	31	31	NUM
eurjchem-479	5	25	december	december	PROPN
eurjchem-479	5	26	2011	2011	NUM
eurjchem-479	5	27	keywords	keyword	NOUN
eurjchem-479	5	28	n‐phenylsulphonyloxytetrachlorophthalimide	n‐phenylsulphonyloxytetrachlorophthalimide	ADV
eurjchem-479	5	29	was	be	AUX
eurjchem-479	5	30	obtained	obtain	VERB
eurjchem-479	5	31	by	by	ADP
eurjchem-479	5	32	treatment	treatment	NOUN
eurjchem-479	5	33	of	of	ADP
eurjchem-479	5	34	n‐hydroxy	n‐hydroxy	PUNCT
eurjchem-479	5	35	tetrachlorophthalimide	tetrachlorophthalimide	ADV
eurjchem-479	5	36	with	with	ADP
eurjchem-479	5	37	benzenesulphonyl	benzenesulphonyl	ADJ
eurjchem-479	5	38	chloride	chloride	NOUN
eurjchem-479	5	39	.	.	PUNCT
eurjchem-479	6	1	also	also	ADV
eurjchem-479	6	2	,	,	PUNCT
eurjchem-479	6	3	the	the	DET
eurjchem-479	6	4	titled	title	VERB
eurjchem-479	6	5	compound	compound	NOUN
eurjchem-479	6	6	3	3	NUM
eurjchem-479	6	7	was	be	AUX
eurjchem-479	6	8	obtained	obtain	VERB
eurjchem-479	6	9	by	by	ADP
eurjchem-479	6	10	reaction	reaction	NOUN
eurjchem-479	6	11	of	of	ADP
eurjchem-479	6	12	compound	compound	NOUN
eurjchem-479	6	13	2	2	NUM
eurjchem-479	6	14	with	with	ADP
eurjchem-479	6	15	hydrazine	hydrazine	NOUN
eurjchem-479	6	16	hydrate	hydrate	NOUN
eurjchem-479	6	17	via	via	ADP
eurjchem-479	6	18	lossen	lossen	PROPN
eurjchem-479	6	19	rearrangement	rearrangement	NOUN
eurjchem-479	6	20	.	.	PUNCT
eurjchem-479	7	1	compound	compound	NOUN
eurjchem-479	7	2	3	3	NUM
eurjchem-479	7	3	used	use	VERB
eurjchem-479	7	4	as	as	ADP
eurjchem-479	7	5	starting	start	VERB
eurjchem-479	7	6	material	material	NOUN
eurjchem-479	7	7	for	for	ADP
eurjchem-479	7	8	the	the	DET
eurjchem-479	7	9	synthesis	synthesis	NOUN
eurjchem-479	7	10	of	of	ADP
eurjchem-479	7	11	new	new	ADJ
eurjchem-479	7	12	pyrimidine	pyrimidine	NOUN
eurjchem-479	7	13	and	and	CCONJ
eurjchem-479	7	14	quinazolinedione	quinazolinedione	ADJ
eurjchem-479	7	15	derivatives	derivative	NOUN
eurjchem-479	7	16	containing	contain	VERB
eurjchem-479	7	17	four	four	NUM
eurjchem-479	7	18	chlorine	chlorine	NOUN
eurjchem-479	7	19	atoms	atom	NOUN
eurjchem-479	7	20	which	which	PRON
eurjchem-479	7	21	have	have	VERB
eurjchem-479	7	22	pharmacological	pharmacological	ADJ
eurjchem-479	7	23	activity	activity	NOUN
eurjchem-479	7	24	.	.	PUNCT
eurjchem-479	8	1	quinazolinedione	quinazolinedione	ADJ
eurjchem-479	8	2	hydrazine	hydrazine	NOUN
eurjchem-479	8	3	hydrate	hydrate	NOUN
eurjchem-479	8	4	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-479	8	5	tetrachloroquinazolindione	tetrachloroquinazolindione	NOUN
eurjchem-479	8	6	n‐phenylsulphonyloxytetrachlorophthalimide	n‐phenylsulphonyloxytetrachlorophthalimide	ADV
eurjchem-479	8	7	3‐(n‐acetylamino)tetrachloroquinazolindione	3‐(n‐acetylamino)tetrachloroquinazolindione	NUM
eurjchem-479	8	8	1	1	NUM
eurjchem-479	8	9	.	.	PUNCT
eurjchem-479	8	10	introduction	introduction	NOUN
eurjchem-479	8	11	owing	owe	VERB
eurjchem-479	8	12	to	to	ADP
eurjchem-479	8	13	the	the	DET
eurjchem-479	8	14	importance	importance	NOUN
eurjchem-479	8	15	of	of	ADP
eurjchem-479	8	16	tetrachlorophthalimides	tetrachlorophthalimide	NOUN
eurjchem-479	8	17	as	as	ADP
eurjchem-479	8	18	good	good	ADJ
eurjchem-479	8	19	α‐glucosides	α‐glucosides	X
eurjchem-479	8	20	inhibitors	inhibitor	NOUN
eurjchem-479	8	21	that	that	PRON
eurjchem-479	8	22	decrease	decrease	VERB
eurjchem-479	8	23	glucose	glucose	NOUN
eurjchem-479	8	24	level	level	NOUN
eurjchem-479	9	1	[	[	X
eurjchem-479	9	2	1,2	1,2	NUM
eurjchem-479	9	3	]	]	PUNCT
eurjchem-479	9	4	in	in	ADP
eurjchem-479	9	5	blood	blood	NOUN
eurjchem-479	9	6	and	and	CCONJ
eurjchem-479	9	7	their	their	PRON
eurjchem-479	9	8	use	use	NOUN
eurjchem-479	9	9	as	as	ADP
eurjchem-479	9	10	potentially	potentially	ADV
eurjchem-479	9	11	valuable	valuable	ADJ
eurjchem-479	9	12	for	for	ADP
eurjchem-479	9	13	various	various	ADJ
eurjchem-479	9	14	diseases	disease	NOUN
eurjchem-479	9	15	,	,	PUNCT
eurjchem-479	9	16	we	we	PRON
eurjchem-479	9	17	aimed	aim	VERB
eurjchem-479	9	18	in	in	ADP
eurjchem-479	9	19	the	the	DET
eurjchem-479	9	20	present	present	ADJ
eurjchem-479	9	21	study	study	NOUN
eurjchem-479	9	22	to	to	PART
eurjchem-479	9	23	synthesize	synthesize	VERB
eurjchem-479	9	24	another	another	DET
eurjchem-479	9	25	class	class	NOUN
eurjchem-479	9	26	of	of	ADP
eurjchem-479	9	27	new	new	ADJ
eurjchem-479	9	28	tetrachloroheterocyclic	tetrachloroheterocyclic	NOUN
eurjchem-479	9	29	compounds	compound	NOUN
eurjchem-479	9	30	such	such	ADJ
eurjchem-479	9	31	as	as	ADP
eurjchem-479	9	32	tetrachloro	tetrachloro	PROPN
eurjchem-479	9	33	quinazolindione	quinazolindione	NOUN
eurjchem-479	9	34	derivatives	derivative	NOUN
eurjchem-479	9	35	.	.	PUNCT
eurjchem-479	10	1	it	it	PRON
eurjchem-479	10	2	has	have	AUX
eurjchem-479	10	3	been	be	AUX
eurjchem-479	10	4	recently	recently	ADV
eurjchem-479	10	5	shown	show	VERB
eurjchem-479	10	6	that	that	SCONJ
eurjchem-479	10	7	pyrimidines	pyrimidine	NOUN
eurjchem-479	10	8	and	and	CCONJ
eurjchem-479	10	9	quinazolindiones	quinazolindione	NOUN
eurjchem-479	10	10	are	be	AUX
eurjchem-479	10	11	important	important	ADJ
eurjchem-479	10	12	compounds	compound	NOUN
eurjchem-479	10	13	posses	posse	NOUN
eurjchem-479	10	14	pharmacological	pharmacological	ADJ
eurjchem-479	10	15	activity	activity	NOUN
eurjchem-479	10	16	including	include	VERB
eurjchem-479	10	17	use	use	NOUN
eurjchem-479	10	18	as	as	ADP
eurjchem-479	10	19	anticonvul‐	anticonvul‐	PROPN
eurjchem-479	10	20	sant	sant	NOUN
eurjchem-479	10	21	,	,	PUNCT
eurjchem-479	10	22	electroshock	electroshock	NOUN
eurjchem-479	10	23	,	,	PUNCT
eurjchem-479	10	24	pentylenetetrazole	pentylenetetrazole	NOUN
eurjchem-479	10	25	induced	induce	VERB
eurjchem-479	10	26	seizures	seizure	NOUN
eurjchem-479	10	27	in	in	ADP
eurjchem-479	10	28	mice	mouse	NOUN
eurjchem-479	11	1	[	[	X
eurjchem-479	11	2	3	3	NUM
eurjchem-479	11	3	]	]	PUNCT
eurjchem-479	11	4	,	,	PUNCT
eurjchem-479	11	5	sedative	sedative	ADJ
eurjchem-479	11	6	,	,	PUNCT
eurjchem-479	11	7	hypotensive	hypotensive	ADJ
eurjchem-479	11	8	[	[	X
eurjchem-479	11	9	4	4	NUM
eurjchem-479	11	10	]	]	PUNCT
eurjchem-479	11	11	,	,	PUNCT
eurjchem-479	11	12	antinflammatory	antinflammatory	NOUN
eurjchem-479	11	13	,	,	PUNCT
eurjchem-479	11	14	antigonisys	antigonisy	NOUN
eurjchem-479	11	15	[	[	X
eurjchem-479	11	16	5,6	5,6	NUM
eurjchem-479	11	17	]	]	PUNCT
eurjchem-479	11	18	,	,	PUNCT
eurjchem-479	11	19	vasodilator	vasodilator	NOUN
eurjchem-479	11	20	[	[	X
eurjchem-479	11	21	7‐9	7‐9	NOUN
eurjchem-479	11	22	]	]	X
eurjchem-479	11	23	,	,	PUNCT
eurjchem-479	11	24	contractile	contractile	NOUN
eurjchem-479	11	25	smooth	smooth	ADJ
eurjchem-479	11	26	muscles	muscle	NOUN
eurjchem-479	11	27	and	and	CCONJ
eurjchem-479	11	28	posses	posse	NOUN
eurjchem-479	11	29	inhibitory	inhibitory	ADJ
eurjchem-479	11	30	activity	activity	NOUN
eurjchem-479	11	31	toward	toward	ADP
eurjchem-479	11	32	the	the	DET
eurjchem-479	11	33	calcium	calcium	NOUN
eurjchem-479	11	34	independent	independent	ADJ
eurjchem-479	11	35	phosphor‐	phosphor‐	NOUN
eurjchem-479	11	36	diesteras	diestera	VERB
eurjchem-479	11	37	enzyme	enzyme	NOUN
eurjchem-479	11	38	[	[	X
eurjchem-479	11	39	10	10	NUM
eurjchem-479	11	40	]	]	PUNCT
eurjchem-479	11	41	.	.	PUNCT
eurjchem-479	12	1	this	this	PRON
eurjchem-479	12	2	encouraged	encourage	VERB
eurjchem-479	12	3	us	we	PRON
eurjchem-479	12	4	to	to	PART
eurjchem-479	12	5	synthesize	synthesize	VERB
eurjchem-479	12	6	quinazolinedione	quinazolinedione	ADJ
eurjchem-479	12	7	derivatives	derivative	NOUN
eurjchem-479	12	8	containing	contain	VERB
eurjchem-479	12	9	four	four	NUM
eurjchem-479	12	10	chlorine	chlorine	NOUN
eurjchem-479	12	11	atoms	atom	NOUN
eurjchem-479	12	12	in	in	ADP
eurjchem-479	12	13	benzene	benzene	NOUN
eurjchem-479	12	14	ring	ring	NOUN
eurjchem-479	12	15	starting	start	VERB
eurjchem-479	12	16	with	with	ADP
eurjchem-479	12	17	tetrachlorophthalic	tetrachlorophthalic	ADJ
eurjchem-479	12	18	anhydride	anhydride	NOUN
eurjchem-479	12	19	which	which	PRON
eurjchem-479	12	20	may	may	AUX
eurjchem-479	12	21	possess	possess	VERB
eurjchem-479	12	22	greater	great	ADJ
eurjchem-479	12	23	certain	certain	ADJ
eurjchem-479	12	24	pharmacological	pharmacological	ADJ
eurjchem-479	12	25	activities	activity	NOUN
eurjchem-479	12	26	.	.	PUNCT
eurjchem-479	13	1	2	2	X
eurjchem-479	13	2	.	.	X
eurjchem-479	13	3	experimental	experimental	ADJ
eurjchem-479	13	4	2.1	2.1	NUM
eurjchem-479	13	5	.	.	PUNCT
eurjchem-479	14	1	instrumentation	instrumentation	NOUN
eurjchem-479	14	2	melting	melting	NOUN
eurjchem-479	14	3	points	point	NOUN
eurjchem-479	14	4	were	be	AUX
eurjchem-479	14	5	uncorrected	uncorrecte	VERB
eurjchem-479	14	6	determined	determined	ADJ
eurjchem-479	14	7	on	on	ADP
eurjchem-479	14	8	an	an	DET
eurjchem-479	14	9	electric	electric	ADJ
eurjchem-479	14	10	melting	melting	NOUN
eurjchem-479	14	11	point	point	NOUN
eurjchem-479	14	12	apparatus	apparatus	NOUN
eurjchem-479	14	13	(	(	PUNCT
eurjchem-479	14	14	kofler	kofler	NOUN
eurjchem-479	14	15	)	)	PUNCT
eurjchem-479	14	16	.	.	PUNCT
eurjchem-479	15	1	the	the	PRON
eurjchem-479	15	2	ir	ir	PROPN
eurjchem-479	15	3	spectra	spectra	PROPN
eurjchem-479	15	4	(	(	PUNCT
eurjchem-479	15	5	kbr	kbr	PROPN
eurjchem-479	15	6	)	)	PUNCT
eurjchem-479	15	7	were	be	AUX
eurjchem-479	15	8	recorded	record	VERB
eurjchem-479	15	9	on	on	ADP
eurjchem-479	15	10	a	a	DET
eurjchem-479	15	11	shimadzu	shimadzu	ADJ
eurjchem-479	15	12	408	408	NUM
eurjchem-479	15	13	spectrometer	spectrometer	NOUN
eurjchem-479	15	14	.	.	PUNCT
eurjchem-479	16	1	the	the	DET
eurjchem-479	16	2	1h	1h	NUM
eurjchem-479	16	3	nmr	nmr	NOUN
eurjchem-479	16	4	spectra	spectra	NOUN
eurjchem-479	16	5	were	be	AUX
eurjchem-479	16	6	recorded	record	VERB
eurjchem-479	16	7	by	by	ADP
eurjchem-479	16	8	200	200	NUM
eurjchem-479	16	9	mhz	mhz	NOUN
eurjchem-479	16	10	varian	varian	NOUN
eurjchem-479	16	11	em	em	PRON
eurjchem-479	16	12	390	390	NUM
eurjchem-479	16	13	spectrometer	spectrometer	NOUN
eurjchem-479	16	14	;	;	PUNCT
eurjchem-479	16	15	chemical	chemical	ADJ
eurjchem-479	16	16	shifts	shift	NOUN
eurjchem-479	16	17	are	be	AUX
eurjchem-479	16	18	reported	report	VERB
eurjchem-479	16	19	in	in	ADP
eurjchem-479	16	20	ppm	ppm	NOUN
eurjchem-479	16	21	with	with	ADP
eurjchem-479	16	22	tms	tms	PROPN
eurjchem-479	16	23	as	as	ADP
eurjchem-479	16	24	an	an	DET
eurjchem-479	16	25	internal	internal	ADJ
eurjchem-479	16	26	standard	standard	NOUN
eurjchem-479	16	27	and	and	CCONJ
eurjchem-479	16	28	are	be	AUX
eurjchem-479	16	29	given	give	VERB
eurjchem-479	16	30	in	in	ADP
eurjchem-479	16	31	δ	δ	PROPN
eurjchem-479	16	32	units	unit	NOUN
eurjchem-479	16	33	.	.	PUNCT
eurjchem-479	17	1	electron	electron	PROPN
eurjchem-479	17	2	impact	impact	PROPN
eurjchem-479	17	3	mass	mass	PROPN
eurjchem-479	17	4	spectra	spectra	NOUN
eurjchem-479	17	5	were	be	AUX
eurjchem-479	17	6	obtained	obtain	VERB
eurjchem-479	17	7	at	at	ADP
eurjchem-479	17	8	70	70	NUM
eurjchem-479	17	9	ev	ev	VERB
eurjchem-479	17	10	using	use	VERB
eurjchem-479	17	11	a	a	DET
eurjchem-479	17	12	gc‐ms	gc‐ms	NOUN
eurjchem-479	17	13	sp.1000	sp.1000	NUM
eurjchem-479	17	14	shimadzu	shimadzu	NOUN
eurjchem-479	17	15	.	.	PUNCT
eurjchem-479	18	1	elemental	elemental	ADJ
eurjchem-479	18	2	analyses	analysis	NOUN
eurjchem-479	18	3	were	be	AUX
eurjchem-479	18	4	carried	carry	VERB
eurjchem-479	18	5	out	out	ADP
eurjchem-479	18	6	at	at	ADP
eurjchem-479	18	7	microanalysis	microanalysis	ADJ
eurjchem-479	18	8	unit	unit	NOUN
eurjchem-479	18	9	at	at	ADP
eurjchem-479	18	10	cairo	cairo	PROPN
eurjchem-479	18	11	university	university	PROPN
eurjchem-479	18	12	;	;	PUNCT
eurjchem-479	18	13	purity	purity	NOUN
eurjchem-479	18	14	of	of	ADP
eurjchem-479	18	15	the	the	DET
eurjchem-479	18	16	compounds	compound	NOUN
eurjchem-479	18	17	was	be	AUX
eurjchem-479	18	18	detected	detect	VERB
eurjchem-479	18	19	by	by	ADP
eurjchem-479	18	20	tlc	tlc	PROPN
eurjchem-479	18	21	.	.	PUNCT
eurjchem-479	19	1	2.2	2.2	NUM
eurjchem-479	19	2	.	.	PUNCT
eurjchem-479	20	1	synthesis	synthesis	NOUN
eurjchem-479	20	2	2.2.1	2.2.1	NUM
eurjchem-479	20	3	.	.	PUNCT
eurjchem-479	20	4	n‐phenylsulphonyloxytetrachlorophthalimide	n‐phenylsulphonyloxytetrachlorophthalimide	PUNCT
eurjchem-479	21	1	(	(	PUNCT
eurjchem-479	21	2	2	2	X
eurjchem-479	21	3	)	)	PUNCT
eurjchem-479	21	4	benzenesulphonyl	benzenesulphonyl	ADJ
eurjchem-479	21	5	chloride	chloride	NOUN
eurjchem-479	21	6	was	be	AUX
eurjchem-479	21	7	added	add	VERB
eurjchem-479	21	8	dropwisely	dropwisely	ADV
eurjchem-479	21	9	with	with	ADP
eurjchem-479	21	10	stirring	stir	VERB
eurjchem-479	21	11	in	in	ADP
eurjchem-479	21	12	ice	ice	NOUN
eurjchem-479	21	13	bath	bath	NOUN
eurjchem-479	21	14	to	to	ADP
eurjchem-479	21	15	a	a	DET
eurjchem-479	21	16	solution	solution	NOUN
eurjchem-479	21	17	of	of	ADP
eurjchem-479	21	18	n‐hydroxytetrachloro	n‐hydroxytetrachloro	SYM
eurjchem-479	21	19	phthalimide	phthalimide	NOUN
eurjchem-479	21	20	(	(	PUNCT
eurjchem-479	21	21	6.3	6.3	NUM
eurjchem-479	21	22	g	g	NOUN
eurjchem-479	21	23	,	,	PUNCT
eurjchem-479	21	24	20	20	NUM
eurjchem-479	21	25	mmol	mmol	NOUN
eurjchem-479	21	26	)	)	PUNCT
eurjchem-479	21	27	in	in	ADP
eurjchem-479	21	28	pyridine	pyridine	NOUN
eurjchem-479	21	29	(	(	PUNCT
eurjchem-479	21	30	15	15	NUM
eurjchem-479	21	31	ml	ml	NOUN
eurjchem-479	21	32	)	)	PUNCT
eurjchem-479	22	1	[	[	X
eurjchem-479	22	2	11	11	NUM
eurjchem-479	22	3	]	]	PUNCT
eurjchem-479	22	4	.	.	PUNCT
eurjchem-479	23	1	the	the	DET
eurjchem-479	23	2	reaction	reaction	NOUN
eurjchem-479	23	3	mixture	mixture	NOUN
eurjchem-479	23	4	was	be	AUX
eurjchem-479	23	5	vigorously	vigorously	ADV
eurjchem-479	23	6	stirred	stir	VERB
eurjchem-479	23	7	for	for	ADP
eurjchem-479	23	8	15	15	NUM
eurjchem-479	23	9	min	min	NOUN
eurjchem-479	23	10	.	.	PROPN
eurjchem-479	23	11	,	,	PUNCT
eurjchem-479	23	12	the	the	DET
eurjchem-479	23	13	solid	solid	ADJ
eurjchem-479	23	14	formed	form	VERB
eurjchem-479	23	15	was	be	AUX
eurjchem-479	23	16	acidified	acidify	VERB
eurjchem-479	23	17	with	with	ADP
eurjchem-479	23	18	cold	cold	ADJ
eurjchem-479	23	19	dilute	dilute	NOUN
eurjchem-479	23	20	hydrochloric	hydrochloric	ADJ
eurjchem-479	23	21	acid	acid	NOUN
eurjchem-479	23	22	(	(	PUNCT
eurjchem-479	23	23	1:1	1:1	NUM
eurjchem-479	23	24	)	)	PUNCT
eurjchem-479	23	25	,	,	PUNCT
eurjchem-479	23	26	and	and	CCONJ
eurjchem-479	23	27	the	the	DET
eurjchem-479	23	28	solid	solid	ADJ
eurjchem-479	23	29	formed	form	VERB
eurjchem-479	23	30	was	be	AUX
eurjchem-479	23	31	filtered	filter	VERB
eurjchem-479	23	32	off	off	ADP
eurjchem-479	23	33	and	and	CCONJ
eurjchem-479	23	34	dried	dry	VERB
eurjchem-479	23	35	.	.	PUNCT
eurjchem-479	24	1	the	the	DET
eurjchem-479	24	2	target	target	NOUN
eurjchem-479	24	3	product	product	NOUN
eurjchem-479	24	4	was	be	AUX
eurjchem-479	24	5	crystallized	crystallize	VERB
eurjchem-479	24	6	from	from	ADP
eurjchem-479	24	7	petroleum	petroleum	NOUN
eurjchem-479	24	8	ether	ether	NOUN
eurjchem-479	24	9	(	(	PUNCT
eurjchem-479	24	10	80‐100	80‐100	NUM
eurjchem-479	24	11	)	)	PUNCT
eurjchem-479	24	12	and	and	CCONJ
eurjchem-479	24	13	benzene	benzene	NOUN
eurjchem-479	24	14	(	(	PUNCT
eurjchem-479	24	15	3:1	3:1	NUM
eurjchem-479	24	16	)	)	PUNCT
eurjchem-479	24	17	to	to	PART
eurjchem-479	24	18	give	give	VERB
eurjchem-479	24	19	n‐phenylsulphonyloxytetrachlorophthal‐	n‐phenylsulphonyloxytetrachlorophthal‐	ADP
eurjchem-479	24	20	imide	imide	NOUN
eurjchem-479	24	21	(	(	PUNCT
eurjchem-479	24	22	3	3	NUM
eurjchem-479	24	23	g	g	NOUN
eurjchem-479	24	24	,	,	PUNCT
eurjchem-479	24	25	6.8	6.8	NUM
eurjchem-479	24	26	mmol	mmol	NOUN
eurjchem-479	24	27	)	)	PUNCT
eurjchem-479	24	28	2	2	NUM
eurjchem-479	24	29	in	in	ADP
eurjchem-479	24	30	yield	yield	NOUN
eurjchem-479	24	31	35	35	NUM
eurjchem-479	24	32	%	%	NOUN
eurjchem-479	24	33	as	as	ADP
eurjchem-479	24	34	yellow	yellow	ADJ
eurjchem-479	24	35	crystals	crystal	NOUN
eurjchem-479	24	36	(	(	PUNCT
eurjchem-479	24	37	scheme	scheme	NOUN
eurjchem-479	24	38	1	1	NUM
eurjchem-479	24	39	)	)	PUNCT
eurjchem-479	24	40	.	.	PUNCT
eurjchem-479	25	1	m.p	m.p	PROPN
eurjchem-479	25	2	.	.	PROPN
eurjchem-479	25	3	:	:	PUNCT
eurjchem-479	26	1	244	244	NUM
eurjchem-479	26	2	oc	oc	NOUN
eurjchem-479	26	3	.	.	PUNCT
eurjchem-479	26	4	ft‐ir	ft‐ir	NOUN
eurjchem-479	26	5	(	(	PUNCT
eurjchem-479	26	6	kbr	kbr	PROPN
eurjchem-479	26	7	,	,	PUNCT
eurjchem-479	26	8	cm‐1	cm‐1	PROPN
eurjchem-479	26	9	):	):	PUNCT
eurjchem-479	26	10	1808	1808	NUM
eurjchem-479	26	11	and	and	CCONJ
eurjchem-479	26	12	1750	1750	NUM
eurjchem-479	26	13	(	(	PUNCT
eurjchem-479	26	14	c	c	NOUN
eurjchem-479	26	15	=	=	NOUN
eurjchem-479	26	16	o	o	NOUN
eurjchem-479	26	17	)	)	PUNCT
eurjchem-479	26	18	,	,	PUNCT
eurjchem-479	26	19	1360	1360	NUM
eurjchem-479	26	20	and	and	CCONJ
eurjchem-479	26	21	1180	1180	NUM
eurjchem-479	26	22	(	(	PUNCT
eurjchem-479	26	23	so2‐o‐	so2‐o‐	NUM
eurjchem-479	26	24	)	)	PUNCT
eurjchem-479	26	25	.	.	PUNCT
eurjchem-479	27	1	1h	1h	NUM
eurjchem-479	27	2	nmr	nmr	NOUN
eurjchem-479	27	3	(	(	PUNCT
eurjchem-479	27	4	300	300	NUM
eurjchem-479	27	5	mhz	mhz	NOUN
eurjchem-479	27	6	,	,	PUNCT
eurjchem-479	27	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-479	27	8	,	,	PUNCT
eurjchem-479	27	9	ppm	ppm	NOUN
eurjchem-479	27	10	):	):	PUNCT
eurjchem-479	27	11	7.70‐	7.70‐	NUM
eurjchem-479	27	12	8.11	8.11	NUM
eurjchem-479	27	13	(	(	PUNCT
eurjchem-479	27	14	m	m	PROPN
eurjchem-479	27	15	,	,	PUNCT
eurjchem-479	27	16	5h	5h	NUM
eurjchem-479	27	17	,	,	PUNCT
eurjchem-479	27	18	ph‐so2	ph‐so2	NOUN
eurjchem-479	27	19	)	)	PUNCT
eurjchem-479	27	20	.	.	PUNCT
eurjchem-479	28	1	ms	ms	NOUN
eurjchem-479	28	2	(	(	PUNCT
eurjchem-479	28	3	m	m	PROPN
eurjchem-479	28	4	/	/	SYM
eurjchem-479	28	5	z	z	NOUN
eurjchem-479	28	6	,	,	PUNCT
eurjchem-479	28	7	%	%	INTJ
eurjchem-479	28	8	):	):	PUNCT
eurjchem-479	28	9	439	439	NUM
eurjchem-479	28	10	(	(	PUNCT
eurjchem-479	28	11	1.01	1.01	NUM
eurjchem-479	28	12	%	%	NOUN
eurjchem-479	28	13	)	)	PUNCT
eurjchem-479	28	14	correspond	correspond	VERB
eurjchem-479	28	15	to	to	ADP
eurjchem-479	28	16	the	the	DET
eurjchem-479	28	17	molecular	molecular	ADJ
eurjchem-479	28	18	formula	formula	NOUN
eurjchem-479	28	19	(	(	PUNCT
eurjchem-479	28	20	c14h5cl4no5s	c14h5cl4no5s	NUM
eurjchem-479	28	21	)	)	PUNCT
eurjchem-479	28	22	in	in	ADP
eurjchem-479	28	23	addition	addition	NOUN
eurjchem-479	28	24	to	to	ADP
eurjchem-479	28	25	the	the	DET
eurjchem-479	28	26	characteristic	characteristic	ADJ
eurjchem-479	28	27	peaks	peak	NOUN
eurjchem-479	28	28	for	for	ADP
eurjchem-479	28	29	compounds	compound	NOUN
eurjchem-479	28	30	containing	contain	VERB
eurjchem-479	28	31	four	four	NUM
eurjchem-479	28	32	chlorine	chlorine	NOUN
eurjchem-479	28	33	atoms	atom	NOUN
eurjchem-479	28	34	[	[	X
eurjchem-479	28	35	13	13	NUM
eurjchem-479	28	36	]	]	PUNCT
eurjchem-479	28	37	at	at	ADP
eurjchem-479	28	38	(	(	PUNCT
eurjchem-479	28	39	m+2	m+2	NOUN
eurjchem-479	28	40	)	)	PUNCT
eurjchem-479	28	41	,	,	PUNCT
eurjchem-479	28	42	(	(	PUNCT
eurjchem-479	28	43	m+4	m+4	ADJ
eurjchem-479	28	44	)	)	PUNCT
eurjchem-479	28	45	and	and	CCONJ
eurjchem-479	28	46	(	(	PUNCT
eurjchem-479	28	47	m+6	m+6	NOUN
eurjchem-479	28	48	)	)	PUNCT
eurjchem-479	28	49	.	.	PUNCT
eurjchem-479	29	1	anal	anal	PROPN
eurjchem-479	29	2	.	.	PUNCT
eurjchem-479	29	3	calcd	calcd	NOUN
eurjchem-479	29	4	.	.	PUNCT
eurjchem-479	30	1	for	for	ADP
eurjchem-479	30	2	c14h5cl4no5s	c14h5cl4no5s	NUM
eurjchem-479	30	3	:	:	PUNCT
eurjchem-479	30	4	c	c	NOUN
eurjchem-479	30	5	,	,	PUNCT
eurjchem-479	30	6	38.12	38.12	NUM
eurjchem-479	30	7	;	;	PUNCT
eurjchem-479	30	8	h	h	X
eurjchem-479	30	9	,	,	PUNCT
eurjchem-479	30	10	1.14	1.14	NUM
eurjchem-479	30	11	;	;	PUNCT
eurjchem-479	30	12	n	n	CCONJ
eurjchem-479	30	13	,	,	PUNCT
eurjchem-479	30	14	3.18	3.18	NUM
eurjchem-479	30	15	.	.	PUNCT
eurjchem-479	30	16	found	find	VERB
eurjchem-479	30	17	:	:	PUNCT
eurjchem-479	31	1	c	c	X
eurjchem-479	31	2	,	,	PUNCT
eurjchem-479	31	3	38.31	38.31	NUM
eurjchem-479	31	4	;	;	PUNCT
eurjchem-479	31	5	h	h	NOUN
eurjchem-479	31	6	,	,	PUNCT
eurjchem-479	31	7	1.16	1.16	NUM
eurjchem-479	31	8	;	;	PUNCT
eurjchem-479	31	9	n	n	CCONJ
eurjchem-479	31	10	,	,	PUNCT
eurjchem-479	31	11	3.18	3.18	NUM
eurjchem-479	31	12	%	%	NOUN
eurjchem-479	31	13	.	.	PUNCT
eurjchem-479	32	1	2.2.2	2.2.2	X
eurjchem-479	32	2	.	.	X
eurjchem-479	33	1	3‐aminotetrachloroquinazolin‐2,4‐dione	3‐aminotetrachloroquinazolin‐2,4‐dione	NUM
eurjchem-479	33	2	(	(	PUNCT
eurjchem-479	33	3	3	3	X
eurjchem-479	33	4	)	)	PUNCT
eurjchem-479	33	5	a	a	DET
eurjchem-479	33	6	mixture	mixture	NOUN
eurjchem-479	33	7	of	of	ADP
eurjchem-479	33	8	n‐phenylsulphonyloxytetrachlorophthalimide	n‐phenylsulphonyloxytetrachlorophthalimide	ADP
eurjchem-479	33	9	,	,	PUNCT
eurjchem-479	33	10	2	2	NUM
eurjchem-479	33	11	,	,	PUNCT
eurjchem-479	33	12	(	(	PUNCT
eurjchem-479	33	13	4.41	4.41	NUM
eurjchem-479	33	14	g	g	NOUN
eurjchem-479	33	15	,	,	PUNCT
eurjchem-479	33	16	10	10	NUM
eurjchem-479	33	17	mmole	mmole	NOUN
eurjchem-479	33	18	)	)	PUNCT
eurjchem-479	33	19	and	and	CCONJ
eurjchem-479	33	20	hydrazine	hydrazine	NOUN
eurjchem-479	33	21	hydrate	hydrate	NOUN
eurjchem-479	33	22	in	in	ADP
eurjchem-479	33	23	dry	dry	ADJ
eurjchem-479	33	24	benzene	benzene	NOUN
eurjchem-479	33	25	(	(	PUNCT
eurjchem-479	33	26	40	40	NUM
eurjchem-479	33	27	ml	ml	NOUN
eurjchem-479	33	28	)	)	PUNCT
eurjchem-479	33	29	using	use	VERB
eurjchem-479	33	30	dean	dean	PROPN
eurjchem-479	33	31	&	&	CCONJ
eurjchem-479	33	32	starks	starks	PROPN
eurjchem-479	33	33	'	'	PART
eurjchem-479	33	34	apparatus	apparatus	NOUN
eurjchem-479	33	35	was	be	AUX
eurjchem-479	33	36	refluxed	refluxe	VERB
eurjchem-479	33	37	for	for	ADP
eurjchem-479	33	38	2	2	NUM
eurjchem-479	33	39	hours	hour	NOUN
eurjchem-479	33	40	[	[	X
eurjchem-479	33	41	12	12	NUM
eurjchem-479	33	42	]	]	PUNCT
eurjchem-479	33	43	.	.	PUNCT
eurjchem-479	34	1	after	after	ADP
eurjchem-479	34	2	cooling	cool	VERB
eurjchem-479	34	3	;	;	PUNCT
eurjchem-479	34	4	the	the	DET
eurjchem-479	34	5	solid	solid	ADJ
eurjchem-479	34	6	formed	form	VERB
eurjchem-479	34	7	was	be	AUX
eurjchem-479	34	8	filtered	filter	VERB
eurjchem-479	34	9	off	off	ADP
eurjchem-479	34	10	and	and	CCONJ
eurjchem-479	34	11	crystallized	crystallize	VERB
eurjchem-479	34	12	from	from	ADP
eurjchem-479	34	13	water	water	NOUN
eurjchem-479	34	14	to	to	PART
eurjchem-479	34	15	give	give	VERB
eurjchem-479	34	16	3‐aminotetrachloroquinazolin‐	3‐aminotetrachloroquinazolin‐	NUM
eurjchem-479	34	17	2,4‐dione	2,4‐dione	NUM
eurjchem-479	34	18	(	(	PUNCT
eurjchem-479	34	19	2.4	2.4	NUM
eurjchem-479	34	20	g	g	NOUN
eurjchem-479	34	21	,	,	PUNCT
eurjchem-479	34	22	7.6	7.6	NUM
eurjchem-479	34	23	mmole	mmole	NOUN
eurjchem-479	34	24	)	)	PUNCT
eurjchem-479	34	25	3	3	NUM
eurjchem-479	34	26	in	in	ADP
eurjchem-479	34	27	yield	yield	NOUN
eurjchem-479	34	28	76	76	NUM
eurjchem-479	34	29	%	%	NOUN
eurjchem-479	34	30	as	as	ADP
eurjchem-479	34	31	white	white	PROPN
eurjchem-479	34	32	crystal	crystal	NOUN
eurjchem-479	34	33	(	(	PUNCT
eurjchem-479	34	34	scheme	scheme	NOUN
eurjchem-479	34	35	2	2	NUM
eurjchem-479	34	36	)	)	PUNCT
eurjchem-479	34	37	.	.	PUNCT
eurjchem-479	35	1	m.p	m.p	PROPN
eurjchem-479	35	2	.	.	PROPN
eurjchem-479	35	3	:	:	PUNCT
eurjchem-479	35	4	274	274	NUM
eurjchem-479	35	5	oc	oc	NOUN
eurjchem-479	35	6	.	.	PUNCT
eurjchem-479	35	7	ft‐ir	ft‐ir	NOUN
eurjchem-479	35	8	(	(	PUNCT
eurjchem-479	35	9	kbr	kbr	PROPN
eurjchem-479	35	10	,	,	PUNCT
eurjchem-479	35	11	cm‐1	cm‐1	PROPN
eurjchem-479	35	12	):	):	PUNCT
eurjchem-479	35	13	3457	3457	NUM
eurjchem-479	35	14	(	(	PUNCT
eurjchem-479	35	15	nh	nh	NOUN
eurjchem-479	35	16	)	)	PUNCT
eurjchem-479	35	17	,	,	PUNCT
eurjchem-479	35	18	3313	3313	NUM
eurjchem-479	35	19	and	and	CCONJ
eurjchem-479	35	20	3206	3206	NUM
eurjchem-479	35	21	(	(	PUNCT
eurjchem-479	35	22	nh2	nh2	PROPN
eurjchem-479	35	23	)	)	PUNCT
eurjchem-479	35	24	,	,	PUNCT
eurjchem-479	35	25	1726	1726	NUM
eurjchem-479	35	26	and	and	CCONJ
eurjchem-479	35	27	1675	1675	NUM
eurjchem-479	35	28	(	(	PUNCT
eurjchem-479	35	29	c	c	NOUN
eurjchem-479	35	30	=	=	NOUN
eurjchem-479	35	31	o	o	NOUN
eurjchem-479	35	32	)	)	PUNCT
eurjchem-479	35	33	.	.	PUNCT
eurjchem-479	36	1	1h	1h	NUM
eurjchem-479	36	2	nmr	nmr	NOUN
eurjchem-479	36	3	(	(	PUNCT
eurjchem-479	36	4	200	200	NUM
eurjchem-479	36	5	mhz	mhz	NOUN
eurjchem-479	36	6	,	,	PUNCT
eurjchem-479	36	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-479	36	8	,	,	PUNCT
eurjchem-479	36	9	ppm	ppm	NOUN
eurjchem-479	36	10	):	):	PUNCT
eurjchem-479	36	11	5.62	5.62	NUM
eurjchem-479	36	12	(	(	PUNCT
eurjchem-479	36	13	s	s	PROPN
eurjchem-479	36	14	,	,	PUNCT
eurjchem-479	36	15	2h	2h	NUM
eurjchem-479	36	16	,	,	PUNCT
eurjchem-479	36	17	nh2	nh2	PROPN
eurjchem-479	36	18	)	)	PUNCT
eurjchem-479	36	19	and	and	CCONJ
eurjchem-479	36	20	also	also	ADV
eurjchem-479	36	21	showed	show	VERB
eurjchem-479	36	22	the	the	DET
eurjchem-479	36	23	disappearance	disappearance	NOUN
eurjchem-479	36	24	of	of	ADP
eurjchem-479	36	25	nh	nh	PROPN
eurjchem-479	36	26	signal	signal	NOUN
eurjchem-479	36	27	in	in	ADP
eurjchem-479	36	28	dmso‐d6	dmso‐d6	PROPN
eurjchem-479	36	29	while	while	SCONJ
eurjchem-479	36	30	ft‐ir	ft‐ir	NOUN
eurjchem-479	36	31	spectrum	spectrum	NOUN
eurjchem-479	36	32	revealed	reveal	VERB
eurjchem-479	36	33	the	the	DET
eurjchem-479	36	34	presence	presence	NOUN
eurjchem-479	36	35	of	of	ADP
eurjchem-479	36	36	a	a	DET
eurjchem-479	36	37	band	band	NOUN
eurjchem-479	36	38	for	for	ADP
eurjchem-479	36	39	νnh	νnh	NOUN
eurjchem-479	36	40	at	at	ADP
eurjchem-479	36	41	3457	3457	NUM
eurjchem-479	36	42	cm‐1	cm‐1	NOUN
eurjchem-479	36	43	.	.	PUNCT
eurjchem-479	37	1	hassan	hassan	PROPN
eurjchem-479	37	2	et	et	PROPN
eurjchem-479	37	3	al	al	PROPN
eurjchem-479	37	4	.	.	PUNCT
eurjchem-479	37	5	/	/	SYM
eurjchem-479	37	6	european	european	PROPN
eurjchem-479	37	7	journal	journal	PROPN
eurjchem-479	37	8	of	of	ADP
eurjchem-479	37	9	chemistry	chemistry	NOUN
eurjchem-479	37	10	2	2	NUM
eurjchem-479	37	11	(	(	PUNCT
eurjchem-479	37	12	4	4	NUM
eurjchem-479	37	13	)	)	PUNCT
eurjchem-479	37	14	(	(	PUNCT
eurjchem-479	37	15	2011	2011	NUM
eurjchem-479	37	16	)	)	PUNCT
eurjchem-479	37	17	514‐518	514‐518	NOUN
eurjchem-479	37	18	515	515	NUM
eurjchem-479	37	19	scheme	scheme	NOUN
eurjchem-479	37	20	1	1	NUM
eurjchem-479	37	21	scheme	scheme	NOUN
eurjchem-479	37	22	2	2	NUM
eurjchem-479	37	23	anal	anal	NOUN
eurjchem-479	37	24	.	.	PUNCT
eurjchem-479	38	1	calcd	calcd	NOUN
eurjchem-479	38	2	.	.	PUNCT
eurjchem-479	39	1	for	for	ADP
eurjchem-479	39	2	c8h3cl4n3o2	c8h3cl4n3o2	NOUN
eurjchem-479	39	3	:	:	PUNCT
eurjchem-479	39	4	c	c	NOUN
eurjchem-479	39	5	,	,	PUNCT
eurjchem-479	39	6	30.52	30.52	NUM
eurjchem-479	39	7	;	;	PUNCT
eurjchem-479	39	8	h	h	NOUN
eurjchem-479	39	9	,	,	PUNCT
eurjchem-479	39	10	0.96	0.96	NUM
eurjchem-479	39	11	;	;	PUNCT
eurjchem-479	39	12	n	n	CCONJ
eurjchem-479	39	13	,	,	PUNCT
eurjchem-479	39	14	13.34	13.34	NUM
eurjchem-479	39	15	.	.	PUNCT
eurjchem-479	39	16	found	find	VERB
eurjchem-479	39	17	:	:	PUNCT
eurjchem-479	40	1	c	c	X
eurjchem-479	40	2	,	,	PUNCT
eurjchem-479	40	3	30.75	30.75	NUM
eurjchem-479	40	4	;	;	PUNCT
eurjchem-479	40	5	h	h	X
eurjchem-479	40	6	,	,	PUNCT
eurjchem-479	40	7	0.97	0.97	NUM
eurjchem-479	40	8	;	;	PUNCT
eurjchem-479	40	9	n	n	CCONJ
eurjchem-479	40	10	,	,	PUNCT
eurjchem-479	40	11	13.34	13.34	NUM
eurjchem-479	40	12	%	%	NOUN
eurjchem-479	40	13	.	.	PUNCT
eurjchem-479	41	1	2.2.3	2.2.3	X
eurjchem-479	41	2	.	.	X
eurjchem-479	42	1	3‐(n‐acetylamino)tetrachloroquinazolin‐2,4‐dione	3‐(n‐acetylamino)tetrachloroquinazolin‐2,4‐dione	NUM
eurjchem-479	42	2	(	(	PUNCT
eurjchem-479	42	3	4	4	NUM
eurjchem-479	42	4	)	)	PUNCT
eurjchem-479	42	5	to	to	ADP
eurjchem-479	42	6	a	a	DET
eurjchem-479	42	7	solution	solution	NOUN
eurjchem-479	42	8	of	of	ADP
eurjchem-479	42	9	3‐aminotetrachloroquinazolin‐2,4‐dione	3‐aminotetrachloroquinazolin‐2,4‐dione	NUM
eurjchem-479	42	10	3	3	NUM
eurjchem-479	42	11	(	(	PUNCT
eurjchem-479	42	12	0.315	0.315	NUM
eurjchem-479	42	13	g	g	NOUN
eurjchem-479	42	14	,	,	PUNCT
eurjchem-479	42	15	1	1	NUM
eurjchem-479	42	16	mmole	mmole	NOUN
eurjchem-479	42	17	)	)	PUNCT
eurjchem-479	42	18	in	in	ADP
eurjchem-479	42	19	dry	dry	ADJ
eurjchem-479	42	20	pyridine	pyridine	NOUN
eurjchem-479	42	21	(	(	PUNCT
eurjchem-479	42	22	10	10	NUM
eurjchem-479	42	23	ml	ml	NOUN
eurjchem-479	42	24	)	)	PUNCT
eurjchem-479	42	25	,	,	PUNCT
eurjchem-479	42	26	acetylchloride	acetylchloride	X
eurjchem-479	42	27	(	(	PUNCT
eurjchem-479	42	28	1	1	NUM
eurjchem-479	42	29	ml	ml	NOUN
eurjchem-479	42	30	)	)	PUNCT
eurjchem-479	42	31	was	be	AUX
eurjchem-479	42	32	added	add	VERB
eurjchem-479	42	33	drop	drop	NOUN
eurjchem-479	42	34	wisely	wisely	ADV
eurjchem-479	42	35	at	at	ADP
eurjchem-479	42	36	room	room	NOUN
eurjchem-479	42	37	temperature	temperature	NOUN
eurjchem-479	42	38	.	.	PUNCT
eurjchem-479	43	1	the	the	DET
eurjchem-479	43	2	reaction	reaction	NOUN
eurjchem-479	43	3	mixture	mixture	NOUN
eurjchem-479	43	4	was	be	AUX
eurjchem-479	43	5	stirred	stir	VERB
eurjchem-479	43	6	for	for	ADP
eurjchem-479	43	7	2	2	NUM
eurjchem-479	43	8	hours	hour	NOUN
eurjchem-479	43	9	,	,	PUNCT
eurjchem-479	43	10	and	and	CCONJ
eurjchem-479	43	11	a	a	DET
eurjchem-479	43	12	cold	cold	ADJ
eurjchem-479	43	13	diluted	dilute	VERB
eurjchem-479	43	14	hcl	hcl	PROPN
eurjchem-479	43	15	(	(	PUNCT
eurjchem-479	43	16	1:1	1:1	NUM
eurjchem-479	43	17	)	)	PUNCT
eurjchem-479	43	18	was	be	AUX
eurjchem-479	43	19	added	add	VERB
eurjchem-479	43	20	to	to	ADP
eurjchem-479	43	21	the	the	DET
eurjchem-479	43	22	reaction	reaction	NOUN
eurjchem-479	43	23	mixture	mixture	NOUN
eurjchem-479	43	24	and	and	CCONJ
eurjchem-479	43	25	the	the	DET
eurjchem-479	43	26	solid	solid	ADJ
eurjchem-479	43	27	formed	form	VERB
eurjchem-479	43	28	was	be	AUX
eurjchem-479	43	29	filtered	filter	VERB
eurjchem-479	43	30	off	off	ADP
eurjchem-479	43	31	and	and	CCONJ
eurjchem-479	43	32	crystallized	crystallize	VERB
eurjchem-479	43	33	from	from	ADP
eurjchem-479	43	34	benzene	benzene	NOUN
eurjchem-479	43	35	/	/	SYM
eurjchem-479	43	36	ethanol	ethanol	NOUN
eurjchem-479	43	37	to	to	PART
eurjchem-479	43	38	give	give	VERB
eurjchem-479	43	39	3‐(n‐acetylamino)tetrachloroquinazolin‐2,4‐dione	3‐(n‐acetylamino)tetrachloroquinazolin‐2,4‐dione	NUM
eurjchem-479	43	40	(	(	PUNCT
eurjchem-479	43	41	0.29	0.29	NUM
eurjchem-479	43	42	g	g	NOUN
eurjchem-479	43	43	,	,	PUNCT
eurjchem-479	43	44	0.81	0.81	NUM
eurjchem-479	43	45	mmole	mmole	NOUN
eurjchem-479	43	46	)	)	PUNCT
eurjchem-479	43	47	4	4	NUM
eurjchem-479	43	48	in	in	ADP
eurjchem-479	43	49	yield	yield	NOUN
eurjchem-479	43	50	81	81	NUM
eurjchem-479	43	51	%	%	NOUN
eurjchem-479	43	52	as	as	ADP
eurjchem-479	43	53	white	white	PROPN
eurjchem-479	43	54	crystal	crystal	NOUN
eurjchem-479	43	55	(	(	PUNCT
eurjchem-479	43	56	scheme	scheme	NOUN
eurjchem-479	43	57	3	3	NUM
eurjchem-479	43	58	)	)	PUNCT
eurjchem-479	43	59	.	.	PUNCT
eurjchem-479	44	1	m.p	m.p	PROPN
eurjchem-479	44	2	.	.	PROPN
eurjchem-479	44	3	:	:	PUNCT
eurjchem-479	45	1	306	306	NUM
eurjchem-479	45	2	oc	oc	NOUN
eurjchem-479	45	3	.	.	PUNCT
eurjchem-479	45	4	ft‐ir	ft‐ir	NOUN
eurjchem-479	45	5	(	(	PUNCT
eurjchem-479	45	6	kbr	kbr	PROPN
eurjchem-479	45	7	,	,	PUNCT
eurjchem-479	45	8	cm‐1	cm‐1	PROPN
eurjchem-479	45	9	):	):	PUNCT
eurjchem-479	45	10	3200	3200	NUM
eurjchem-479	45	11	(	(	PUNCT
eurjchem-479	45	12	nh	nh	NOUN
eurjchem-479	45	13	)	)	PUNCT
eurjchem-479	45	14	,	,	PUNCT
eurjchem-479	45	15	1780	1780	NUM
eurjchem-479	45	16	and	and	CCONJ
eurjchem-479	45	17	1750	1750	NUM
eurjchem-479	45	18	(	(	PUNCT
eurjchem-479	45	19	c	c	NOUN
eurjchem-479	45	20	=	=	NOUN
eurjchem-479	45	21	o	o	NOUN
eurjchem-479	45	22	)	)	PUNCT
eurjchem-479	45	23	(	(	PUNCT
eurjchem-479	45	24	imide	imide	NOUN
eurjchem-479	45	25	carbonyl	carbonyl	NOUN
eurjchem-479	45	26	)	)	PUNCT
eurjchem-479	45	27	.	.	PUNCT
eurjchem-479	46	1	1h	1h	NUM
eurjchem-479	46	2	nmr	nmr	NOUN
eurjchem-479	46	3	(	(	PUNCT
eurjchem-479	46	4	200	200	NUM
eurjchem-479	46	5	mhz	mhz	NOUN
eurjchem-479	46	6	,	,	PUNCT
eurjchem-479	46	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-479	46	8	,	,	PUNCT
eurjchem-479	46	9	ppm	ppm	NOUN
eurjchem-479	46	10	):	):	PUNCT
eurjchem-479	46	11	1.93	1.93	NUM
eurjchem-479	46	12	(	(	PUNCT
eurjchem-479	46	13	s	s	PROPN
eurjchem-479	46	14	,	,	PUNCT
eurjchem-479	46	15	3h	3h	NUM
eurjchem-479	46	16	,	,	PUNCT
eurjchem-479	46	17	ch3	ch3	PROPN
eurjchem-479	46	18	)	)	PUNCT
eurjchem-479	46	19	,	,	PUNCT
eurjchem-479	46	20	10.6	10.6	NUM
eurjchem-479	46	21	(	(	PUNCT
eurjchem-479	46	22	s	s	PROPN
eurjchem-479	46	23	,	,	PUNCT
eurjchem-479	46	24	1h	1h	NUM
eurjchem-479	46	25	,	,	PUNCT
eurjchem-479	46	26	nh	nh	PROPN
eurjchem-479	46	27	)	)	PUNCT
eurjchem-479	46	28	,	,	PUNCT
eurjchem-479	46	29	11.4	11.4	NUM
eurjchem-479	46	30	(	(	PUNCT
eurjchem-479	46	31	s	s	PROPN
eurjchem-479	46	32	,	,	PUNCT
eurjchem-479	46	33	1h	1h	NUM
eurjchem-479	46	34	,	,	PUNCT
eurjchem-479	46	35	nh	nh	PROPN
eurjchem-479	46	36	)	)	PUNCT
eurjchem-479	46	37	.	.	PUNCT
eurjchem-479	47	1	anal	anal	PROPN
eurjchem-479	47	2	.	.	PUNCT
eurjchem-479	47	3	calcd	calcd	NOUN
eurjchem-479	47	4	.	.	PUNCT
eurjchem-479	48	1	for	for	ADP
eurjchem-479	48	2	c10h5cl4n3o3	c10h5cl4n3o3	NOUN
eurjchem-479	48	3	:	:	PUNCT
eurjchem-479	48	4	c	c	X
eurjchem-479	48	5	,	,	PUNCT
eurjchem-479	48	6	33.65	33.65	NUM
eurjchem-479	48	7	;	;	PUNCT
eurjchem-479	48	8	h	h	NOUN
eurjchem-479	48	9	,	,	PUNCT
eurjchem-479	48	10	1.41	1.41	NUM
eurjchem-479	48	11	;	;	PUNCT
eurjchem-479	48	12	n	n	CCONJ
eurjchem-479	48	13	,	,	PUNCT
eurjchem-479	48	14	11.77	11.77	NUM
eurjchem-479	48	15	.	.	PUNCT
eurjchem-479	49	1	found	find	VERB
eurjchem-479	49	2	:	:	PUNCT
eurjchem-479	50	1	c	c	X
eurjchem-479	50	2	,	,	PUNCT
eurjchem-479	50	3	33.86	33.86	NUM
eurjchem-479	50	4	;	;	PUNCT
eurjchem-479	50	5	h	h	NOUN
eurjchem-479	50	6	,	,	PUNCT
eurjchem-479	50	7	1.42	1.42	NUM
eurjchem-479	50	8	;	;	PUNCT
eurjchem-479	50	9	n	n	CCONJ
eurjchem-479	50	10	,	,	PUNCT
eurjchem-479	50	11	11.98	11.98	NUM
eurjchem-479	50	12	%	%	NOUN
eurjchem-479	50	13	.	.	PUNCT
eurjchem-479	51	1	2.2.4	2.2.4	NUM
eurjchem-479	51	2	.	.	X
eurjchem-479	52	1	3‐(phenylsulphonylamino)tetrachloroquinazolin‐2,4‐	3‐(phenylsulphonylamino)tetrachloroquinazolin‐2,4‐	NUM
eurjchem-479	52	2	dione	dione	NOUN
eurjchem-479	52	3	(	(	PUNCT
eurjchem-479	52	4	5	5	NUM
eurjchem-479	52	5	)	)	PUNCT
eurjchem-479	52	6	3‐aminotetrachloroquinazolin‐2,4‐dione	3‐aminotetrachloroquinazolin‐2,4‐dione	NUM
eurjchem-479	52	7	3	3	NUM
eurjchem-479	52	8	(	(	PUNCT
eurjchem-479	52	9	0.31	0.31	NUM
eurjchem-479	52	10	g	g	NOUN
eurjchem-479	52	11	,	,	PUNCT
eurjchem-479	52	12	1	1	NUM
eurjchem-479	52	13	mmole	mmole	NOUN
eurjchem-479	52	14	)	)	PUNCT
eurjchem-479	52	15	in	in	ADP
eurjchem-479	52	16	dry	dry	ADJ
eurjchem-479	52	17	pyridine	pyridine	NOUN
eurjchem-479	52	18	(	(	PUNCT
eurjchem-479	52	19	10	10	NUM
eurjchem-479	52	20	ml	ml	NOUN
eurjchem-479	52	21	)	)	PUNCT
eurjchem-479	52	22	was	be	AUX
eurjchem-479	52	23	cooled	cool	VERB
eurjchem-479	52	24	in	in	ADP
eurjchem-479	52	25	ice	ice	NOUN
eurjchem-479	52	26	bath	bath	NOUN
eurjchem-479	52	27	;	;	PUNCT
eurjchem-479	52	28	benzenesulphonyl	benzenesulphonyl	PROPN
eurjchem-479	52	29	chloride	chloride	NOUN
eurjchem-479	52	30	was	be	AUX
eurjchem-479	52	31	added	add	VERB
eurjchem-479	52	32	drop	drop	NOUN
eurjchem-479	52	33	wisely	wisely	ADV
eurjchem-479	52	34	.	.	PUNCT
eurjchem-479	53	1	the	the	DET
eurjchem-479	53	2	reaction	reaction	NOUN
eurjchem-479	53	3	mixture	mixture	NOUN
eurjchem-479	53	4	with	with	ADP
eurjchem-479	53	5	stirred	stir	VERB
eurjchem-479	53	6	at	at	ADP
eurjchem-479	53	7	room	room	NOUN
eurjchem-479	53	8	temperature	temperature	NOUN
eurjchem-479	53	9	for	for	ADP
eurjchem-479	53	10	4	4	NUM
eurjchem-479	53	11	hours	hour	NOUN
eurjchem-479	53	12	.	.	PUNCT
eurjchem-479	54	1	a	a	DET
eurjchem-479	54	2	cold	cold	ADJ
eurjchem-479	54	3	diluted	dilute	VERB
eurjchem-479	54	4	hcl	hcl	PROPN
eurjchem-479	54	5	(	(	PUNCT
eurjchem-479	54	6	1:1	1:1	NUM
eurjchem-479	54	7	)	)	PUNCT
eurjchem-479	54	8	was	be	AUX
eurjchem-479	54	9	added	add	VERB
eurjchem-479	54	10	to	to	ADP
eurjchem-479	54	11	the	the	DET
eurjchem-479	54	12	reaction	reaction	NOUN
eurjchem-479	54	13	mixture	mixture	NOUN
eurjchem-479	54	14	and	and	CCONJ
eurjchem-479	54	15	the	the	DET
eurjchem-479	54	16	solid	solid	ADJ
eurjchem-479	54	17	formed	form	VERB
eurjchem-479	54	18	was	be	AUX
eurjchem-479	54	19	filtered	filter	VERB
eurjchem-479	54	20	off	off	ADP
eurjchem-479	54	21	and	and	CCONJ
eurjchem-479	54	22	crystallized	crystallize	VERB
eurjchem-479	54	23	from	from	ADP
eurjchem-479	54	24	benzene	benzene	NOUN
eurjchem-479	54	25	/	/	SYM
eurjchem-479	54	26	ethanol	ethanol	NOUN
eurjchem-479	54	27	to	to	PART
eurjchem-479	54	28	give	give	VERB
eurjchem-479	54	29	3‐(phenylsulphonylamino)tetrachloro	3‐(phenylsulphonylamino)tetrachloro	NUM
eurjchem-479	54	30	quinazolin‐2,4,dione	quinazolin‐2,4,dione	NOUN
eurjchem-479	54	31	(	(	PUNCT
eurjchem-479	54	32	0.27	0.27	NUM
eurjchem-479	54	33	g	g	NOUN
eurjchem-479	54	34	,	,	PUNCT
eurjchem-479	54	35	0.59	0.59	NUM
eurjchem-479	54	36	mmole	mmole	NOUN
eurjchem-479	54	37	)	)	PUNCT
eurjchem-479	54	38	5	5	NUM
eurjchem-479	54	39	in	in	ADP
eurjchem-479	54	40	yield	yield	NOUN
eurjchem-479	54	41	59	59	NUM
eurjchem-479	54	42	%	%	NOUN
eurjchem-479	54	43	as	as	ADP
eurjchem-479	54	44	yellow	yellow	ADJ
eurjchem-479	54	45	crystal	crystal	NOUN
eurjchem-479	54	46	(	(	PUNCT
eurjchem-479	54	47	scheme	scheme	NOUN
eurjchem-479	54	48	3	3	NUM
eurjchem-479	54	49	)	)	PUNCT
eurjchem-479	54	50	.	.	PUNCT
eurjchem-479	55	1	m.p	m.p	PROPN
eurjchem-479	55	2	.	.	PROPN
eurjchem-479	55	3	:	:	PUNCT
eurjchem-479	56	1	300	300	NUM
eurjchem-479	56	2	oc	oc	NOUN
eurjchem-479	56	3	.	.	PUNCT
eurjchem-479	56	4	ft‐ir	ft‐ir	NOUN
eurjchem-479	56	5	(	(	PUNCT
eurjchem-479	56	6	kbr	kbr	PROPN
eurjchem-479	56	7	,	,	PUNCT
eurjchem-479	56	8	cm‐1	cm‐1	PROPN
eurjchem-479	56	9	):	):	PUNCT
eurjchem-479	56	10	3200	3200	NUM
eurjchem-479	56	11	(	(	PUNCT
eurjchem-479	56	12	nh	nh	NOUN
eurjchem-479	56	13	)	)	PUNCT
eurjchem-479	56	14	,	,	PUNCT
eurjchem-479	56	15	1810	1810	NUM
eurjchem-479	56	16	,	,	PUNCT
eurjchem-479	56	17	1750	1750	NUM
eurjchem-479	56	18	(	(	PUNCT
eurjchem-479	56	19	c	c	NOUN
eurjchem-479	56	20	=	=	NOUN
eurjchem-479	56	21	o	o	NOUN
eurjchem-479	56	22	)	)	PUNCT
eurjchem-479	56	23	,	,	PUNCT
eurjchem-479	56	24	1360	1360	NUM
eurjchem-479	56	25	,	,	PUNCT
eurjchem-479	56	26	1180	1180	NUM
eurjchem-479	56	27	(	(	PUNCT
eurjchem-479	56	28	so2	so2	NOUN
eurjchem-479	56	29	)	)	PUNCT
eurjchem-479	56	30	.	.	PUNCT
eurjchem-479	57	1	1h	1h	NUM
eurjchem-479	57	2	nmr	nmr	NOUN
eurjchem-479	57	3	(	(	PUNCT
eurjchem-479	57	4	200	200	NUM
eurjchem-479	57	5	mhz	mhz	NOUN
eurjchem-479	57	6	,	,	PUNCT
eurjchem-479	57	7	dmso‐d6	dmso‐d6	NUM
eurjchem-479	57	8	):	):	PUNCT
eurjchem-479	57	9	7.30‐7.90	7.30‐7.90	NUM
eurjchem-479	57	10	(	(	PUNCT
eurjchem-479	57	11	m	m	PROPN
eurjchem-479	57	12	,	,	PUNCT
eurjchem-479	57	13	5h	5h	NUM
eurjchem-479	57	14	,	,	PUNCT
eurjchem-479	57	15	ar‐h	ar‐h	NOUN
eurjchem-479	57	16	)	)	PUNCT
eurjchem-479	57	17	,	,	PUNCT
eurjchem-479	57	18	9.75	9.75	NUM
eurjchem-479	57	19	(	(	PUNCT
eurjchem-479	57	20	s	s	PROPN
eurjchem-479	57	21	,	,	PUNCT
eurjchem-479	57	22	1h	1h	NUM
eurjchem-479	57	23	,	,	PUNCT
eurjchem-479	57	24	nh	nh	PROPN
eurjchem-479	57	25	)	)	PUNCT
eurjchem-479	57	26	,	,	PUNCT
eurjchem-479	57	27	11.40	11.40	NUM
eurjchem-479	57	28	(	(	PUNCT
eurjchem-479	57	29	s	s	PROPN
eurjchem-479	57	30	,	,	PUNCT
eurjchem-479	57	31	1h	1h	NUM
eurjchem-479	57	32	,	,	PUNCT
eurjchem-479	57	33	nh	nh	PROPN
eurjchem-479	57	34	)	)	PUNCT
eurjchem-479	57	35	.	.	PUNCT
eurjchem-479	58	1	anal	anal	PROPN
eurjchem-479	58	2	.	.	PUNCT
eurjchem-479	58	3	calcd	calcd	NOUN
eurjchem-479	58	4	.	.	PUNCT
eurjchem-479	59	1	for	for	ADP
eurjchem-479	59	2	c14h7cl4	c14h7cl4	PROPN
eurjchem-479	59	3	n3o4s	n3o4s	PUNCT
eurjchem-479	59	4	.	.	PUNCT
eurjchem-479	60	1	c	c	X
eurjchem-479	60	2	,	,	PUNCT
eurjchem-479	60	3	36.95	36.95	NUM
eurjchem-479	60	4	;	;	PUNCT
eurjchem-479	60	5	h	h	NOUN
eurjchem-479	60	6	,	,	PUNCT
eurjchem-479	60	7	1.55	1.55	NUM
eurjchem-479	60	8	;	;	PUNCT
eurjchem-479	60	9	n	n	CCONJ
eurjchem-479	60	10	,	,	PUNCT
eurjchem-479	60	11	9.23	9.23	NUM
eurjchem-479	60	12	.	.	PUNCT
eurjchem-479	60	13	found	find	VERB
eurjchem-479	60	14	:	:	PUNCT
eurjchem-479	61	1	c	c	X
eurjchem-479	61	2	,	,	PUNCT
eurjchem-479	61	3	37.23	37.23	NUM
eurjchem-479	61	4	;	;	PUNCT
eurjchem-479	61	5	h	h	X
eurjchem-479	61	6	,	,	PUNCT
eurjchem-479	61	7	1.56	1.56	NUM
eurjchem-479	61	8	;	;	PUNCT
eurjchem-479	61	9	n	n	CCONJ
eurjchem-479	61	10	,	,	PUNCT
eurjchem-479	61	11	9.34	9.34	NUM
eurjchem-479	61	12	%	%	NOUN
eurjchem-479	61	13	.	.	PUNCT
eurjchem-479	62	1	2.2.5	2.2.5	X
eurjchem-479	62	2	.	.	X
eurjchem-479	62	3	3‐(2‐thiophenecarbonylamino)tetrachloroquinazolin‐	3‐(2‐thiophenecarbonylamino)tetrachloroquinazolin‐	NUM
eurjchem-479	62	4	2,4‐dione	2,4‐dione	NUM
eurjchem-479	62	5	(	(	PUNCT
eurjchem-479	62	6	6	6	NUM
eurjchem-479	62	7	)	)	PUNCT
eurjchem-479	62	8	a	a	DET
eurjchem-479	62	9	solution	solution	NOUN
eurjchem-479	62	10	of	of	ADP
eurjchem-479	62	11	3‐aminotetrachloroquinazolin‐2,4‐dione	3‐aminotetrachloroquinazolin‐2,4‐dione	NUM
eurjchem-479	62	12	3	3	NUM
eurjchem-479	62	13	(	(	PUNCT
eurjchem-479	62	14	0.31	0.31	NUM
eurjchem-479	62	15	g	g	NOUN
eurjchem-479	62	16	,	,	PUNCT
eurjchem-479	62	17	1	1	NUM
eurjchem-479	62	18	mmole	mmole	NOUN
eurjchem-479	62	19	)	)	PUNCT
eurjchem-479	62	20	in	in	ADP
eurjchem-479	62	21	dry	dry	ADJ
eurjchem-479	62	22	pyridine	pyridine	NOUN
eurjchem-479	62	23	(	(	PUNCT
eurjchem-479	62	24	10	10	NUM
eurjchem-479	62	25	ml	ml	NOUN
eurjchem-479	62	26	)	)	PUNCT
eurjchem-479	62	27	was	be	AUX
eurjchem-479	62	28	cooled	cool	VERB
eurjchem-479	62	29	in	in	ADP
eurjchem-479	62	30	ice	ice	NOUN
eurjchem-479	62	31	bath	bath	NOUN
eurjchem-479	62	32	;	;	PUNCT
eurjchem-479	62	33	2‐thiophenecarbonyl	2‐thiophenecarbonyl	NUM
eurjchem-479	62	34	chloride	chloride	NOUN
eurjchem-479	62	35	was	be	AUX
eurjchem-479	62	36	added	add	VERB
eurjchem-479	62	37	drop	drop	NOUN
eurjchem-479	62	38	wisely	wisely	ADV
eurjchem-479	62	39	with	with	ADP
eurjchem-479	62	40	stirring	stir	VERB
eurjchem-479	62	41	for	for	ADP
eurjchem-479	62	42	4	4	NUM
eurjchem-479	62	43	hours	hour	NOUN
eurjchem-479	62	44	.	.	PUNCT
eurjchem-479	63	1	a	a	DET
eurjchem-479	63	2	cold	cold	ADJ
eurjchem-479	63	3	diluted	dilute	VERB
eurjchem-479	63	4	hcl	hcl	PROPN
eurjchem-479	63	5	(	(	PUNCT
eurjchem-479	63	6	1:1	1:1	NUM
eurjchem-479	63	7	)	)	PUNCT
eurjchem-479	63	8	was	be	AUX
eurjchem-479	63	9	added	add	VERB
eurjchem-479	63	10	to	to	ADP
eurjchem-479	63	11	the	the	DET
eurjchem-479	63	12	reaction	reaction	NOUN
eurjchem-479	63	13	mixture	mixture	NOUN
eurjchem-479	63	14	and	and	CCONJ
eurjchem-479	63	15	the	the	DET
eurjchem-479	63	16	solid	solid	ADJ
eurjchem-479	63	17	formed	form	VERB
eurjchem-479	63	18	was	be	AUX
eurjchem-479	63	19	filtered	filter	VERB
eurjchem-479	63	20	off	off	ADP
eurjchem-479	63	21	and	and	CCONJ
eurjchem-479	63	22	crystallized	crystallize	VERB
eurjchem-479	63	23	from	from	ADP
eurjchem-479	63	24	benzene	benzene	NOUN
eurjchem-479	63	25	/	/	SYM
eurjchem-479	63	26	ethanol	ethanol	NOUN
eurjchem-479	63	27	to	to	PART
eurjchem-479	63	28	give	give	VERB
eurjchem-479	63	29	3‐(2‐thiophene‐	3‐(2‐thiophene‐	NUM
eurjchem-479	63	30	carbonylamino)tetrachloroquinazolin‐2,4‐dione	carbonylamino)tetrachloroquinazolin‐2,4‐dione	X
eurjchem-479	63	31	(	(	PUNCT
eurjchem-479	63	32	0.28	0.28	NUM
eurjchem-479	63	33	g	g	NOUN
eurjchem-479	63	34	,	,	PUNCT
eurjchem-479	63	35	0.729	0.729	NUM
eurjchem-479	63	36	mmole	mmole	NOUN
eurjchem-479	63	37	)	)	PUNCT
eurjchem-479	63	38	6	6	NUM
eurjchem-479	63	39	in	in	ADP
eurjchem-479	63	40	yield	yield	NOUN
eurjchem-479	63	41	67	67	NUM
eurjchem-479	63	42	%	%	NOUN
eurjchem-479	63	43	as	as	ADP
eurjchem-479	63	44	white	white	PROPN
eurjchem-479	63	45	crystal	crystal	NOUN
eurjchem-479	63	46	(	(	PUNCT
eurjchem-479	63	47	scheme	scheme	NOUN
eurjchem-479	63	48	3	3	NUM
eurjchem-479	63	49	)	)	PUNCT
eurjchem-479	63	50	.	.	PUNCT
eurjchem-479	64	1	m.p	m.p	PROPN
eurjchem-479	64	2	.	.	PROPN
eurjchem-479	64	3	:	:	PUNCT
eurjchem-479	64	4	308	308	NUM
eurjchem-479	64	5	oc	oc	NOUN
eurjchem-479	64	6	.	.	PUNCT
eurjchem-479	64	7	ft‐ir	ft‐ir	NOUN
eurjchem-479	64	8	(	(	PUNCT
eurjchem-479	64	9	kbr	kbr	PROPN
eurjchem-479	64	10	,	,	PUNCT
eurjchem-479	64	11	cm‐1	cm‐1	PROPN
eurjchem-479	64	12	):	):	PUNCT
eurjchem-479	64	13	3200	3200	NUM
eurjchem-479	64	14	(	(	PUNCT
eurjchem-479	64	15	nh	nh	NOUN
eurjchem-479	64	16	)	)	PUNCT
eurjchem-479	64	17	,	,	PUNCT
eurjchem-479	64	18	1740	1740	NUM
eurjchem-479	64	19	and	and	CCONJ
eurjchem-479	64	20	1680	1680	NUM
eurjchem-479	64	21	(	(	PUNCT
eurjchem-479	64	22	c	c	NOUN
eurjchem-479	64	23	=	=	NOUN
eurjchem-479	64	24	o	o	NOUN
eurjchem-479	64	25	)	)	PUNCT
eurjchem-479	64	26	.	.	PUNCT
eurjchem-479	65	1	1h	1h	NUM
eurjchem-479	65	2	nmr	nmr	NOUN
eurjchem-479	65	3	(	(	PUNCT
eurjchem-479	65	4	200	200	NUM
eurjchem-479	65	5	mhz	mhz	NOUN
eurjchem-479	65	6	,	,	PUNCT
eurjchem-479	65	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-479	65	8	,	,	PUNCT
eurjchem-479	65	9	ppm	ppm	NOUN
eurjchem-479	65	10	):	):	PUNCT
eurjchem-479	65	11	7.26‐7.28	7.26‐7.28	NUM
eurjchem-479	65	12	(	(	PUNCT
eurjchem-479	65	13	dd	dd	PROPN
eurjchem-479	65	14	,	,	PUNCT
eurjchem-479	65	15	1h	1h	NUM
eurjchem-479	65	16	,	,	PUNCT
eurjchem-479	65	17	hx	hx	PROPN
eurjchem-479	65	18	)	)	PUNCT
eurjchem-479	65	19	,	,	PUNCT
eurjchem-479	65	20	7.96	7.96	NUM
eurjchem-479	65	21	(	(	PUNCT
eurjchem-479	65	22	dd	dd	PROPN
eurjchem-479	65	23	,	,	PUNCT
eurjchem-479	65	24	1h	1h	NUM
eurjchem-479	65	25	,	,	PUNCT
eurjchem-479	65	26	hm	hm	INTJ
eurjchem-479	65	27	)	)	PUNCT
eurjchem-479	65	28	,	,	PUNCT
eurjchem-479	65	29	7.98‐8.02	7.98‐8.02	NUM
eurjchem-479	65	30	(	(	PUNCT
eurjchem-479	65	31	dd	dd	PROPN
eurjchem-479	65	32	,	,	PUNCT
eurjchem-479	65	33	1h	1h	NUM
eurjchem-479	65	34	,	,	PUNCT
eurjchem-479	65	35	ha	ha	INTJ
eurjchem-479	65	36	)	)	PUNCT
eurjchem-479	65	37	,	,	PUNCT
eurjchem-479	65	38	11.34	11.34	NUM
eurjchem-479	65	39	(	(	PUNCT
eurjchem-479	65	40	s	s	PROPN
eurjchem-479	65	41	,	,	PUNCT
eurjchem-479	65	42	1h	1h	NUM
eurjchem-479	65	43	,	,	PUNCT
eurjchem-479	65	44	nh	nh	PROPN
eurjchem-479	65	45	)	)	PUNCT
eurjchem-479	65	46	,	,	PUNCT
eurjchem-479	65	47	11.55	11.55	NUM
eurjchem-479	65	48	(	(	PUNCT
eurjchem-479	65	49	s	s	PROPN
eurjchem-479	65	50	,	,	PUNCT
eurjchem-479	65	51	1h	1h	NUM
eurjchem-479	65	52	,	,	PUNCT
eurjchem-479	65	53	nh	nh	PROPN
eurjchem-479	65	54	)	)	PUNCT
eurjchem-479	65	55	.	.	PUNCT
eurjchem-479	66	1	ms	ms	NOUN
eurjchem-479	66	2	(	(	PUNCT
eurjchem-479	66	3	m	m	PROPN
eurjchem-479	66	4	/	/	SYM
eurjchem-479	66	5	z	z	NOUN
eurjchem-479	66	6	,	,	PUNCT
eurjchem-479	66	7	%	%	INTJ
eurjchem-479	66	8	):	):	PUNCT
eurjchem-479	66	9	423	423	NUM
eurjchem-479	66	10	(	(	PUNCT
eurjchem-479	66	11	0.59	0.59	NUM
eurjchem-479	66	12	%	%	NOUN
eurjchem-479	66	13	)	)	PUNCT
eurjchem-479	66	14	(	(	PUNCT
eurjchem-479	66	15	m+	m+	NOUN
eurjchem-479	66	16	)	)	PUNCT
eurjchem-479	66	17	in	in	ADP
eurjchem-479	66	18	addition	addition	NOUN
eurjchem-479	66	19	to	to	ADP
eurjchem-479	66	20	the	the	DET
eurjchem-479	66	21	characteristic	characteristic	ADJ
eurjchem-479	66	22	peaks	peak	NOUN
eurjchem-479	66	23	for	for	ADP
eurjchem-479	66	24	compounds	compound	NOUN
eurjchem-479	66	25	containing	contain	VERB
eurjchem-479	66	26	four	four	NUM
eurjchem-479	66	27	chlorine	chlorine	NOUN
eurjchem-479	66	28	atoms	atom	NOUN
eurjchem-479	66	29	at	at	ADP
eurjchem-479	66	30	m	m	PROPN
eurjchem-479	66	31	/	/	SYM
eurjchem-479	66	32	z	z	NOUN
eurjchem-479	66	33	=	=	NOUN
eurjchem-479	66	34	425	425	NUM
eurjchem-479	66	35	(	(	PUNCT
eurjchem-479	66	36	0.66	0.66	NUM
eurjchem-479	66	37	%	%	NOUN
eurjchem-479	66	38	)	)	PUNCT
eurjchem-479	66	39	(	(	PUNCT
eurjchem-479	66	40	m+2	m+2	NOUN
eurjchem-479	66	41	)	)	PUNCT
eurjchem-479	66	42	,	,	PUNCT
eurjchem-479	66	43	427	427	NUM
eurjchem-479	66	44	(	(	PUNCT
eurjchem-479	66	45	0.41	0.41	NUM
eurjchem-479	66	46	%	%	NOUN
eurjchem-479	66	47	)	)	PUNCT
eurjchem-479	66	48	(	(	PUNCT
eurjchem-479	66	49	m+4	m+4	ADJ
eurjchem-479	66	50	)	)	PUNCT
eurjchem-479	66	51	and	and	CCONJ
eurjchem-479	66	52	429	429	NUM
eurjchem-479	66	53	(	(	PUNCT
eurjchem-479	66	54	0.08	0.08	NUM
eurjchem-479	66	55	%	%	NOUN
eurjchem-479	66	56	)	)	PUNCT
eurjchem-479	66	57	(	(	PUNCT
eurjchem-479	66	58	m+6	m+6	NOUN
eurjchem-479	66	59	)	)	PUNCT
eurjchem-479	66	60	.	.	PUNCT
eurjchem-479	67	1	anal	anal	PROPN
eurjchem-479	67	2	.	.	PUNCT
eurjchem-479	67	3	calcd	calcd	NOUN
eurjchem-479	67	4	.	.	PUNCT
eurjchem-479	68	1	for	for	ADP
eurjchem-479	68	2	c13h5cl4n3o3s	c13h5cl4n3o3s	NOUN
eurjchem-479	68	3	:	:	PUNCT
eurjchem-479	68	4	c	c	X
eurjchem-479	68	5	,	,	PUNCT
eurjchem-479	68	6	36.74	36.74	NUM
eurjchem-479	68	7	;	;	PUNCT
eurjchem-479	68	8	h	h	NOUN
eurjchem-479	68	9	,	,	PUNCT
eurjchem-479	68	10	1.18	1.18	NUM
eurjchem-479	68	11	;	;	PUNCT
eurjchem-479	68	12	n	n	CCONJ
eurjchem-479	68	13	,	,	PUNCT
eurjchem-479	68	14	9.88	9.88	NUM
eurjchem-479	68	15	.	.	PUNCT
eurjchem-479	68	16	found	find	VERB
eurjchem-479	68	17	:	:	PUNCT
eurjchem-479	69	1	c	c	X
eurjchem-479	69	2	,	,	PUNCT
eurjchem-479	69	3	36.98	36.98	NUM
eurjchem-479	69	4	;	;	PUNCT
eurjchem-479	69	5	h,1.19	h,1.19	PROPN
eurjchem-479	69	6	;	;	PUNCT
eurjchem-479	69	7	n	n	PRON
eurjchem-479	69	8	10.05	10.05	NUM
eurjchem-479	69	9	%	%	NOUN
eurjchem-479	69	10	.	.	PUNCT
eurjchem-479	70	1	2.2.6	2.2.6	NUM
eurjchem-479	70	2	.	.	NOUN
eurjchem-479	70	3	3‐(2‐chloromethylcarbonylamino)tetrachloro	3‐(2‐chloromethylcarbonylamino)tetrachloro	NUM
eurjchem-479	71	1	quinazolin‐2,4‐dione	quinazolin‐2,4‐dione	NOUN
eurjchem-479	71	2	(	(	PUNCT
eurjchem-479	71	3	7	7	NUM
eurjchem-479	71	4	)	)	PUNCT
eurjchem-479	71	5	to	to	ADP
eurjchem-479	71	6	a	a	DET
eurjchem-479	71	7	stirred	stir	VERB
eurjchem-479	71	8	solution	solution	NOUN
eurjchem-479	71	9	of	of	ADP
eurjchem-479	71	10	3‐aminotetrachloroquinazolin‐2,4‐	3‐aminotetrachloroquinazolin‐2,4‐	NUM
eurjchem-479	71	11	dione	dione	NOUN
eurjchem-479	71	12	3	3	NUM
eurjchem-479	71	13	(	(	PUNCT
eurjchem-479	71	14	0.31	0.31	NUM
eurjchem-479	71	15	g	g	NOUN
eurjchem-479	71	16	,	,	PUNCT
eurjchem-479	71	17	1	1	NUM
eurjchem-479	71	18	mmole	mmole	NOUN
eurjchem-479	71	19	)	)	PUNCT
eurjchem-479	71	20	in	in	ADP
eurjchem-479	71	21	dmf	dmf	PROPN
eurjchem-479	71	22	(	(	PUNCT
eurjchem-479	71	23	10	10	NUM
eurjchem-479	71	24	ml	ml	NOUN
eurjchem-479	71	25	)	)	PUNCT
eurjchem-479	71	26	,	,	PUNCT
eurjchem-479	71	27	chloroacetylchloride	chloroacetylchloride	NOUN
eurjchem-479	71	28	(	(	PUNCT
eurjchem-479	71	29	1	1	NUM
eurjchem-479	71	30	ml	ml	NOUN
eurjchem-479	71	31	)	)	PUNCT
eurjchem-479	71	32	was	be	AUX
eurjchem-479	71	33	added	add	VERB
eurjchem-479	71	34	drop	drop	NOUN
eurjchem-479	71	35	wisely	wisely	ADV
eurjchem-479	71	36	at	at	ADP
eurjchem-479	71	37	room	room	NOUN
eurjchem-479	71	38	temperature	temperature	NOUN
eurjchem-479	71	39	.	.	PUNCT
eurjchem-479	72	1	the	the	DET
eurjchem-479	72	2	reaction	reaction	NOUN
eurjchem-479	72	3	mixture	mixture	NOUN
eurjchem-479	72	4	was	be	AUX
eurjchem-479	72	5	stirred	stir	VERB
eurjchem-479	72	6	for	for	ADP
eurjchem-479	72	7	2	2	NUM
eurjchem-479	72	8	hours	hour	NOUN
eurjchem-479	72	9	,	,	PUNCT
eurjchem-479	72	10	and	and	CCONJ
eurjchem-479	72	11	then	then	ADV
eurjchem-479	72	12	dilute	dilute	VERB
eurjchem-479	72	13	with	with	ADP
eurjchem-479	72	14	cold	cold	ADJ
eurjchem-479	72	15	water	water	NOUN
eurjchem-479	72	16	.	.	PUNCT
eurjchem-479	73	1	the	the	DET
eurjchem-479	73	2	solid	solid	ADJ
eurjchem-479	73	3	formed	form	VERB
eurjchem-479	73	4	was	be	AUX
eurjchem-479	73	5	filtered	filter	VERB
eurjchem-479	73	6	off	off	ADP
eurjchem-479	73	7	and	and	CCONJ
eurjchem-479	73	8	crystallized	crystallize	VERB
eurjchem-479	73	9	from	from	ADP
eurjchem-479	73	10	benzene	benzene	NOUN
eurjchem-479	73	11	/	/	SYM
eurjchem-479	73	12	ethanol	ethanol	NOUN
eurjchem-479	73	13	to	to	PART
eurjchem-479	73	14	give	give	VERB
eurjchem-479	73	15	3‐(2‐chloromethylcarbonyl‐	3‐(2‐chloromethylcarbonyl‐	PRON
eurjchem-479	73	16	amino)tetrachloroquinazolin‐2,4‐dione	amino)tetrachloroquinazolin‐2,4‐dione	NOUN
eurjchem-479	73	17	(	(	PUNCT
eurjchem-479	73	18	0.35	0.35	NUM
eurjchem-479	73	19	g	g	NOUN
eurjchem-479	73	20	,	,	PUNCT
eurjchem-479	73	21	0.89	0.89	NUM
eurjchem-479	73	22	mmole	mmole	NOUN
eurjchem-479	73	23	)	)	PUNCT
eurjchem-479	73	24	7	7	NUM
eurjchem-479	73	25	in	in	ADP
eurjchem-479	73	26	yield	yield	NOUN
eurjchem-479	73	27	89	89	NUM
eurjchem-479	73	28	%	%	NOUN
eurjchem-479	73	29	as	as	ADP
eurjchem-479	73	30	white	white	PROPN
eurjchem-479	73	31	crystal	crystal	NOUN
eurjchem-479	73	32	(	(	PUNCT
eurjchem-479	73	33	scheme	scheme	NOUN
eurjchem-479	73	34	3	3	NUM
eurjchem-479	73	35	)	)	PUNCT
eurjchem-479	73	36	.	.	PUNCT
eurjchem-479	74	1	m.p	m.p	PROPN
eurjchem-479	74	2	.	.	PROPN
eurjchem-479	74	3	:	:	PUNCT
eurjchem-479	74	4	320	320	NUM
eurjchem-479	74	5	oc	oc	NOUN
eurjchem-479	74	6	.	.	PUNCT
eurjchem-479	74	7	ft‐ir	ft‐ir	NOUN
eurjchem-479	74	8	(	(	PUNCT
eurjchem-479	74	9	kbr	kbr	PROPN
eurjchem-479	74	10	,	,	PUNCT
eurjchem-479	74	11	cm‐1	cm‐1	PROPN
eurjchem-479	74	12	):	):	PUNCT
eurjchem-479	74	13	3211	3211	NUM
eurjchem-479	74	14	(	(	PUNCT
eurjchem-479	74	15	nh	nh	NOUN
eurjchem-479	74	16	)	)	PUNCT
eurjchem-479	74	17	,	,	PUNCT
eurjchem-479	74	18	3021	3021	NUM
eurjchem-479	74	19	(	(	PUNCT
eurjchem-479	74	20	ch	ch	NOUN
eurjchem-479	74	21	aliph	aliph	PROPN
eurjchem-479	74	22	.	.	PUNCT
eurjchem-479	74	23	)	)	PUNCT
eurjchem-479	74	24	,	,	PUNCT
eurjchem-479	74	25	1741	1741	NUM
eurjchem-479	74	26	and	and	CCONJ
eurjchem-479	74	27	1700	1700	NUM
eurjchem-479	74	28	(	(	PUNCT
eurjchem-479	74	29	c	c	NOUN
eurjchem-479	74	30	=	=	NOUN
eurjchem-479	74	31	o	o	NOUN
eurjchem-479	74	32	)	)	PUNCT
eurjchem-479	74	33	.	.	PUNCT
eurjchem-479	75	1	1h	1h	NUM
eurjchem-479	75	2	nmr	nmr	NOUN
eurjchem-479	75	3	(	(	PUNCT
eurjchem-479	75	4	200	200	NUM
eurjchem-479	75	5	mhz	mhz	NOUN
eurjchem-479	75	6	,	,	PUNCT
eurjchem-479	75	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-479	75	8	,	,	PUNCT
eurjchem-479	75	9	ppm	ppm	NOUN
eurjchem-479	75	10	):	):	PUNCT
eurjchem-479	75	11	4.04	4.04	NUM
eurjchem-479	75	12	(	(	PUNCT
eurjchem-479	75	13	s	s	PROPN
eurjchem-479	75	14	,	,	PUNCT
eurjchem-479	75	15	2h	2h	NUM
eurjchem-479	75	16	,	,	PUNCT
eurjchem-479	75	17	ch2	ch2	PROPN
eurjchem-479	75	18	)	)	PUNCT
eurjchem-479	75	19	,	,	PUNCT
eurjchem-479	75	20	11.2	11.2	NUM
eurjchem-479	75	21	(	(	PUNCT
eurjchem-479	75	22	s	s	PROPN
eurjchem-479	75	23	,	,	PUNCT
eurjchem-479	75	24	1h	1h	NUM
eurjchem-479	75	25	,	,	PUNCT
eurjchem-479	75	26	nh	nh	PROPN
eurjchem-479	75	27	)	)	PUNCT
eurjchem-479	75	28	,	,	PUNCT
eurjchem-479	75	29	11.58	11.58	NUM
eurjchem-479	75	30	(	(	PUNCT
eurjchem-479	75	31	s	s	PROPN
eurjchem-479	75	32	,	,	PUNCT
eurjchem-479	75	33	1h	1h	NUM
eurjchem-479	75	34	,	,	PUNCT
eurjchem-479	75	35	nh	nh	PROPN
eurjchem-479	75	36	)	)	PUNCT
eurjchem-479	75	37	.	.	PUNCT
eurjchem-479	76	1	anal	anal	PROPN
eurjchem-479	76	2	.	.	PUNCT
eurjchem-479	76	3	calcd	calcd	NOUN
eurjchem-479	76	4	.	.	PUNCT
eurjchem-479	77	1	for	for	ADP
eurjchem-479	77	2	c10h4cl5n3o3	c10h4cl5n3o3	NOUN
eurjchem-479	77	3	:	:	PUNCT
eurjchem-479	77	4	c	c	X
eurjchem-479	77	5	,	,	PUNCT
eurjchem-479	77	6	30.69	30.69	NUM
eurjchem-479	77	7	;	;	PUNCT
eurjchem-479	77	8	h	h	NOUN
eurjchem-479	77	9	,	,	PUNCT
eurjchem-479	77	10	1.03	1.03	NUM
eurjchem-479	77	11	;	;	PUNCT
eurjchem-479	77	12	n	n	CCONJ
eurjchem-479	77	13	,	,	PUNCT
eurjchem-479	77	14	10.73	10.73	NUM
eurjchem-479	77	15	.	.	PUNCT
eurjchem-479	78	1	found	find	VERB
eurjchem-479	78	2	:	:	PUNCT
eurjchem-479	79	1	c	c	X
eurjchem-479	79	2	,	,	PUNCT
eurjchem-479	79	3	30.81	30.81	NUM
eurjchem-479	79	4	;	;	PUNCT
eurjchem-479	79	5	h	h	NOUN
eurjchem-479	79	6	,	,	PUNCT
eurjchem-479	79	7	1.02	1.02	NUM
eurjchem-479	79	8	;	;	PUNCT
eurjchem-479	79	9	n	n	DET
eurjchem-479	79	10	10.90	10.90	NUM
eurjchem-479	79	11	%	%	NOUN
eurjchem-479	79	12	.	.	PUNCT
eurjchem-479	80	1	2.2.7	2.2.7	X
eurjchem-479	80	2	.	.	PUNCT
eurjchem-479	81	1	3‐(n‐benzamido)tetrachloroquinazolin‐2,4‐dione	3‐(n‐benzamido)tetrachloroquinazolin‐2,4‐dione	NUM
eurjchem-479	81	2	(	(	PUNCT
eurjchem-479	81	3	8a	8a	NUM
eurjchem-479	81	4	)	)	PUNCT
eurjchem-479	81	5	a	a	DET
eurjchem-479	81	6	solution	solution	NOUN
eurjchem-479	81	7	of	of	ADP
eurjchem-479	81	8	3‐aminotetrachloroquinazolin‐2,4‐dione	3‐aminotetrachloroquinazolin‐2,4‐dione	NUM
eurjchem-479	81	9	3	3	NUM
eurjchem-479	81	10	(	(	PUNCT
eurjchem-479	81	11	0.31	0.31	NUM
eurjchem-479	81	12	g	g	NOUN
eurjchem-479	81	13	,	,	PUNCT
eurjchem-479	81	14	1	1	NUM
eurjchem-479	81	15	mmole	mmole	NOUN
eurjchem-479	81	16	)	)	PUNCT
eurjchem-479	81	17	in	in	ADP
eurjchem-479	81	18	dry	dry	ADJ
eurjchem-479	81	19	pyridine	pyridine	NOUN
eurjchem-479	81	20	(	(	PUNCT
eurjchem-479	81	21	10	10	NUM
eurjchem-479	81	22	ml	ml	NOUN
eurjchem-479	81	23	)	)	PUNCT
eurjchem-479	81	24	was	be	AUX
eurjchem-479	81	25	cooled	cool	VERB
eurjchem-479	81	26	in	in	ADP
eurjchem-479	81	27	ice	ice	NOUN
eurjchem-479	81	28	bath	bath	NOUN
eurjchem-479	81	29	;	;	PUNCT
eurjchem-479	81	30	benzoylchloride	benzoylchloride	NOUN
eurjchem-479	81	31	was	be	AUX
eurjchem-479	81	32	added	add	VERB
eurjchem-479	81	33	drop	drop	NOUN
eurjchem-479	81	34	wisely	wisely	ADV
eurjchem-479	81	35	with	with	ADP
eurjchem-479	81	36	stirring	stir	VERB
eurjchem-479	81	37	for	for	ADP
eurjchem-479	81	38	4	4	NUM
eurjchem-479	81	39	hours	hour	NOUN
eurjchem-479	81	40	.	.	PUNCT
eurjchem-479	82	1	a	a	DET
eurjchem-479	82	2	cold	cold	ADJ
eurjchem-479	82	3	diluted	dilute	VERB
eurjchem-479	82	4	hcl	hcl	PROPN
eurjchem-479	82	5	(	(	PUNCT
eurjchem-479	82	6	1:1)was	1:1)was	NUM
eurjchem-479	82	7	added	add	VERB
eurjchem-479	82	8	to	to	ADP
eurjchem-479	82	9	the	the	DET
eurjchem-479	82	10	reaction	reaction	NOUN
eurjchem-479	82	11	mixture	mixture	NOUN
eurjchem-479	82	12	and	and	CCONJ
eurjchem-479	82	13	the	the	DET
eurjchem-479	82	14	solid	solid	ADJ
eurjchem-479	82	15	formed	form	VERB
eurjchem-479	82	16	was	be	AUX
eurjchem-479	82	17	filtered	filter	VERB
eurjchem-479	82	18	off	off	ADP
eurjchem-479	82	19	and	and	CCONJ
eurjchem-479	82	20	crystallized	crystallize	VERB
eurjchem-479	82	21	from	from	ADP
eurjchem-479	82	22	benzene	benzene	NOUN
eurjchem-479	82	23	/	/	SYM
eurjchem-479	82	24	ethanol	ethanol	NOUN
eurjchem-479	82	25	to	to	PART
eurjchem-479	82	26	give	give	VERB
eurjchem-479	82	27	3‐(n‐benzamido)tetrachloro	3‐(n‐benzamido)tetrachloro	NUM
eurjchem-479	82	28	quinazolin‐2,4‐dione	quinazolin‐2,4‐dione	PROPN
eurjchem-479	82	29	(	(	PUNCT
eurjchem-479	82	30	0.32	0.32	NUM
eurjchem-479	82	31	g	g	NOUN
eurjchem-479	82	32	,	,	PUNCT
eurjchem-479	82	33	0.76	0.76	NUM
eurjchem-479	82	34	mmole	mmole	NOUN
eurjchem-479	82	35	)	)	PUNCT
eurjchem-479	82	36	8a	8a	NUM
eurjchem-479	82	37	in	in	ADP
eurjchem-479	82	38	yield	yield	NOUN
eurjchem-479	82	39	78	78	NUM
eurjchem-479	82	40	%	%	NOUN
eurjchem-479	82	41	as	as	ADP
eurjchem-479	82	42	white	white	PROPN
eurjchem-479	82	43	crystal	crystal	NOUN
eurjchem-479	82	44	(	(	PUNCT
eurjchem-479	82	45	scheme	scheme	NOUN
eurjchem-479	82	46	3	3	NUM
eurjchem-479	82	47	)	)	PUNCT
eurjchem-479	82	48	.	.	PUNCT
eurjchem-479	83	1	m.p	m.p	PROPN
eurjchem-479	83	2	.	.	PROPN
eurjchem-479	83	3	:	:	PUNCT
eurjchem-479	83	4	310	310	NUM
eurjchem-479	83	5	oc	oc	NOUN
eurjchem-479	83	6	.	.	PUNCT
eurjchem-479	83	7	ft‐ir	ft‐ir	NOUN
eurjchem-479	83	8	(	(	PUNCT
eurjchem-479	83	9	kbr	kbr	PROPN
eurjchem-479	83	10	,	,	PUNCT
eurjchem-479	83	11	cm‐1	cm‐1	PROPN
eurjchem-479	83	12	):	):	PUNCT
eurjchem-479	83	13	3200	3200	NUM
eurjchem-479	83	14	(	(	PUNCT
eurjchem-479	83	15	nh	nh	NOUN
eurjchem-479	83	16	)	)	PUNCT
eurjchem-479	83	17	,	,	PUNCT
eurjchem-479	83	18	3000	3000	NUM
eurjchem-479	83	19	(	(	PUNCT
eurjchem-479	83	20	ch	ch	NOUN
eurjchem-479	83	21	arom	arom	NOUN
eurjchem-479	83	22	.	.	PUNCT
eurjchem-479	83	23	)	)	PUNCT
eurjchem-479	83	24	,	,	PUNCT
eurjchem-479	83	25	1740	1740	NUM
eurjchem-479	83	26	and	and	CCONJ
eurjchem-479	83	27	1660	1660	NUM
eurjchem-479	83	28	(	(	PUNCT
eurjchem-479	83	29	c	c	NOUN
eurjchem-479	83	30	=	=	NOUN
eurjchem-479	83	31	o	o	NOUN
eurjchem-479	83	32	)	)	PUNCT
eurjchem-479	83	33	.	.	PUNCT
eurjchem-479	84	1	1h	1h	NUM
eurjchem-479	84	2	nmr	nmr	NOUN
eurjchem-479	84	3	(	(	PUNCT
eurjchem-479	84	4	200	200	NUM
eurjchem-479	84	5	mhz	mhz	NOUN
eurjchem-479	84	6	,	,	PUNCT
eurjchem-479	84	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-479	84	8	,	,	PUNCT
eurjchem-479	84	9	ppm	ppm	NUM
eurjchem-479	84	10	):	):	PUNCT
eurjchem-479	84	11	7.30‐8.00	7.30‐8.00	PROPN
eurjchem-479	84	12	(	(	PUNCT
eurjchem-479	84	13	m	m	PROPN
eurjchem-479	84	14	,	,	PUNCT
eurjchem-479	84	15	5h	5h	NUM
eurjchem-479	84	16	,	,	PUNCT
eurjchem-479	84	17	ar‐h	ar‐h	NOUN
eurjchem-479	84	18	)	)	PUNCT
eurjchem-479	84	19	,	,	PUNCT
eurjchem-479	84	20	11.30	11.30	NUM
eurjchem-479	84	21	(	(	PUNCT
eurjchem-479	84	22	s	s	PROPN
eurjchem-479	84	23	,	,	PUNCT
eurjchem-479	84	24	1h	1h	NUM
eurjchem-479	84	25	,	,	PUNCT
eurjchem-479	84	26	nh	nh	PROPN
eurjchem-479	84	27	)	)	PUNCT
eurjchem-479	84	28	,	,	PUNCT
eurjchem-479	84	29	11.40	11.40	NUM
eurjchem-479	84	30	(	(	PUNCT
eurjchem-479	84	31	s	s	PROPN
eurjchem-479	84	32	,	,	PUNCT
eurjchem-479	84	33	1h	1h	NUM
eurjchem-479	84	34	,	,	PUNCT
eurjchem-479	84	35	nh	nh	PROPN
eurjchem-479	84	36	)	)	PUNCT
eurjchem-479	84	37	.	.	PUNCT
eurjchem-479	85	1	anal	anal	PROPN
eurjchem-479	85	2	.	.	PUNCT
eurjchem-479	85	3	calcd	calcd	NOUN
eurjchem-479	85	4	.	.	PUNCT
eurjchem-479	86	1	for	for	ADP
eurjchem-479	86	2	c15h7cl4n3o3	c15h7cl4n3o3	NOUN
eurjchem-479	86	3	.	.	PUNCT
eurjchem-479	87	1	c	c	X
eurjchem-479	87	2	,	,	PUNCT
eurjchem-479	87	3	42.99	42.99	NUM
eurjchem-479	87	4	;	;	PUNCT
eurjchem-479	87	5	h	h	NOUN
eurjchem-479	87	6	,	,	PUNCT
eurjchem-479	87	7	1.68	1.68	NUM
eurjchem-479	87	8	;	;	PUNCT
eurjchem-479	87	9	n	n	CCONJ
eurjchem-479	87	10	,	,	PUNCT
eurjchem-479	87	11	10.03	10.03	NUM
eurjchem-479	87	12	.	.	PUNCT
eurjchem-479	87	13	found	find	VERB
eurjchem-479	87	14	:	:	PUNCT
eurjchem-479	88	1	c	c	X
eurjchem-479	88	2	,	,	PUNCT
eurjchem-479	88	3	43.20	43.20	NUM
eurjchem-479	88	4	;	;	PUNCT
eurjchem-479	88	5	h	h	NOUN
eurjchem-479	88	6	,	,	PUNCT
eurjchem-479	88	7	1.66	1.66	NUM
eurjchem-479	88	8	;	;	PUNCT
eurjchem-479	88	9	n	n	DET
eurjchem-479	88	10	10.07	10.07	NUM
eurjchem-479	88	11	%	%	NOUN
eurjchem-479	88	12	.	.	PUNCT
eurjchem-479	89	1	2.2.8	2.2.8	X
eurjchem-479	89	2	.	.	PUNCT
eurjchem-479	90	1	3‐[(n‐(4‐bromobenzamido)tetrachloroquinazolin‐2,4‐	3‐[(n‐(4‐bromobenzamido)tetrachloroquinazolin‐2,4‐	DET
eurjchem-479	90	2	dione	dione	NOUN
eurjchem-479	90	3	(	(	PUNCT
eurjchem-479	90	4	8b	8b	NUM
eurjchem-479	90	5	)	)	PUNCT
eurjchem-479	90	6	a	a	DET
eurjchem-479	90	7	mixture	mixture	NOUN
eurjchem-479	90	8	of	of	ADP
eurjchem-479	90	9	3‐aminotetrachloroquinazolin‐2,4‐dione	3‐aminotetrachloroquinazolin‐2,4‐dione	NUM
eurjchem-479	90	10	3	3	NUM
eurjchem-479	90	11	(	(	PUNCT
eurjchem-479	90	12	0.31	0.31	NUM
eurjchem-479	90	13	g	g	NOUN
eurjchem-479	90	14	,	,	PUNCT
eurjchem-479	90	15	1	1	NUM
eurjchem-479	90	16	mmole	mmole	NOUN
eurjchem-479	90	17	)	)	PUNCT
eurjchem-479	90	18	and	and	CCONJ
eurjchem-479	90	19	p‐bromobenzoylchloride	p‐bromobenzoylchloride	ADP
eurjchem-479	90	20	(	(	PUNCT
eurjchem-479	90	21	0.21	0.21	NUM
eurjchem-479	90	22	g	g	NOUN
eurjchem-479	90	23	,	,	PUNCT
eurjchem-479	90	24	1	1	NUM
eurjchem-479	90	25	mmole	mmole	NOUN
eurjchem-479	90	26	)	)	PUNCT
eurjchem-479	90	27	in	in	ADP
eurjchem-479	90	28	dry	dry	ADJ
eurjchem-479	90	29	pyridine	pyridine	NOUN
eurjchem-479	90	30	(	(	PUNCT
eurjchem-479	90	31	10	10	NUM
eurjchem-479	90	32	ml	ml	NOUN
eurjchem-479	90	33	)	)	PUNCT
eurjchem-479	90	34	was	be	AUX
eurjchem-479	90	35	heated	heat	VERB
eurjchem-479	90	36	under	under	ADP
eurjchem-479	90	37	reflux	reflux	NOUN
eurjchem-479	90	38	for	for	ADP
eurjchem-479	90	39	1/2	1/2	NUM
eurjchem-479	90	40	hour	hour	NOUN
eurjchem-479	90	41	.	.	PUNCT
eurjchem-479	91	1	after	after	ADP
eurjchem-479	91	2	cooling	cool	VERB
eurjchem-479	91	3	,	,	PUNCT
eurjchem-479	91	4	the	the	DET
eurjchem-479	91	5	reaction	reaction	NOUN
eurjchem-479	91	6	mixture	mixture	NOUN
eurjchem-479	91	7	was	be	AUX
eurjchem-479	91	8	poured	pour	VERB
eurjchem-479	91	9	into	into	ADP
eurjchem-479	91	10	cold	cold	ADJ
eurjchem-479	91	11	diluted	dilute	VERB
eurjchem-479	91	12	hcl	hcl	PROPN
eurjchem-479	91	13	(	(	PUNCT
eurjchem-479	91	14	1:1	1:1	NUM
eurjchem-479	91	15	)	)	PUNCT
eurjchem-479	91	16	.	.	PUNCT
eurjchem-479	92	1	the	the	DET
eurjchem-479	92	2	solid	solid	ADJ
eurjchem-479	92	3	formed	form	VERB
eurjchem-479	92	4	was	be	AUX
eurjchem-479	92	5	filtered	filter	VERB
eurjchem-479	92	6	off	off	ADP
eurjchem-479	92	7	and	and	CCONJ
eurjchem-479	92	8	crystallized	crystallize	VERB
eurjchem-479	92	9	from	from	ADP
eurjchem-479	92	10	benzene	benzene	NOUN
eurjchem-479	92	11	/	/	SYM
eurjchem-479	92	12	ethanol	ethanol	NOUN
eurjchem-479	92	13	to	to	PART
eurjchem-479	92	14	give	give	VERB
eurjchem-479	92	15	3‐[(n‐(4‐bromo	3‐[(n‐(4‐bromo	NUM
eurjchem-479	92	16	benzamido)tetrachloroquinazolin‐2,4‐dione	benzamido)tetrachloroquinazolin‐2,4‐dione	NOUN
eurjchem-479	92	17	(	(	PUNCT
eurjchem-479	92	18	0.28	0.28	NUM
eurjchem-479	92	19	g	g	NOUN
eurjchem-479	92	20	,	,	PUNCT
eurjchem-479	92	21	0.56	0.56	NUM
eurjchem-479	92	22	mmole	mmole	NOUN
eurjchem-479	92	23	)	)	PUNCT
eurjchem-479	92	24	8b	8b	PROPN
eurjchem-479	92	25	in	in	ADP
eurjchem-479	92	26	yield	yield	NOUN
eurjchem-479	92	27	56	56	NUM
eurjchem-479	92	28	%	%	NOUN
eurjchem-479	92	29	as	as	ADP
eurjchem-479	92	30	white	white	PROPN
eurjchem-479	92	31	crystal	crystal	NOUN
eurjchem-479	92	32	(	(	PUNCT
eurjchem-479	92	33	scheme	scheme	NOUN
eurjchem-479	92	34	3	3	NUM
eurjchem-479	92	35	)	)	PUNCT
eurjchem-479	92	36	.	.	PUNCT
eurjchem-479	93	1	m.p	m.p	PROPN
eurjchem-479	93	2	.	.	PROPN
eurjchem-479	93	3	:	:	PUNCT
eurjchem-479	93	4	314	314	NUM
eurjchem-479	93	5	oc	oc	NOUN
eurjchem-479	93	6	.	.	PUNCT
eurjchem-479	94	1	516	516	NUM
eurjchem-479	94	2	hassan	hassan	PROPN
eurjchem-479	94	3	et	et	PROPN
eurjchem-479	94	4	al	al	PROPN
eurjchem-479	94	5	.	.	PUNCT
eurjchem-479	94	6	/	/	SYM
eurjchem-479	94	7	european	european	PROPN
eurjchem-479	94	8	journal	journal	PROPN
eurjchem-479	94	9	of	of	ADP
eurjchem-479	94	10	chemistry	chemistry	NOUN
eurjchem-479	94	11	2	2	NUM
eurjchem-479	94	12	(	(	PUNCT
eurjchem-479	94	13	4	4	NUM
eurjchem-479	94	14	)	)	PUNCT
eurjchem-479	94	15	(	(	PUNCT
eurjchem-479	94	16	2011	2011	NUM
eurjchem-479	94	17	)	)	PUNCT
eurjchem-479	94	18	514‐518	514‐518	NOUN
eurjchem-479	94	19	scheme	scheme	NOUN
eurjchem-479	94	20	3	3	NUM
eurjchem-479	94	21	ft‐ir	ft‐ir	NOUN
eurjchem-479	94	22	(	(	PUNCT
eurjchem-479	94	23	kbr	kbr	PROPN
eurjchem-479	94	24	,	,	PUNCT
eurjchem-479	94	25	cm‐1	cm‐1	PROPN
eurjchem-479	94	26	):	):	PUNCT
eurjchem-479	94	27	3200	3200	NUM
eurjchem-479	94	28	(	(	PUNCT
eurjchem-479	94	29	nh	nh	NOUN
eurjchem-479	94	30	)	)	PUNCT
eurjchem-479	94	31	,	,	PUNCT
eurjchem-479	94	32	3000	3000	NUM
eurjchem-479	94	33	(	(	PUNCT
eurjchem-479	94	34	ch	ch	NOUN
eurjchem-479	94	35	arom	arom	NOUN
eurjchem-479	94	36	.	.	PUNCT
eurjchem-479	94	37	)	)	PUNCT
eurjchem-479	94	38	,	,	PUNCT
eurjchem-479	94	39	1740	1740	NUM
eurjchem-479	94	40	and	and	CCONJ
eurjchem-479	94	41	1660	1660	NUM
eurjchem-479	94	42	(	(	PUNCT
eurjchem-479	94	43	c	c	NOUN
eurjchem-479	94	44	=	=	NOUN
eurjchem-479	94	45	o	o	NOUN
eurjchem-479	94	46	)	)	PUNCT
eurjchem-479	94	47	.	.	PUNCT
eurjchem-479	95	1	1h	1h	NUM
eurjchem-479	95	2	nmr	nmr	NOUN
eurjchem-479	95	3	(	(	PUNCT
eurjchem-479	95	4	200	200	NUM
eurjchem-479	95	5	mhz	mhz	NOUN
eurjchem-479	95	6	,	,	PUNCT
eurjchem-479	95	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-479	95	8	,	,	PUNCT
eurjchem-479	95	9	ppm	ppm	NOUN
eurjchem-479	95	10	):	):	PUNCT
eurjchem-479	95	11	7.70‐7.90	7.70‐7.90	NUM
eurjchem-479	95	12	(	(	PUNCT
eurjchem-479	95	13	two	two	NUM
eurjchem-479	95	14	doublet	doublet	ADJ
eurjchem-479	95	15	4h	4h	NOUN
eurjchem-479	95	16	,	,	PUNCT
eurjchem-479	95	17	a2b2	a2b2	PROPN
eurjchem-479	95	18	arom	arom	ADJ
eurjchem-479	95	19	.	.	PUNCT
eurjchem-479	95	20	)	)	PUNCT
eurjchem-479	95	21	,	,	PUNCT
eurjchem-479	95	22	10.65	10.65	NUM
eurjchem-479	95	23	(	(	PUNCT
eurjchem-479	95	24	s	s	PROPN
eurjchem-479	95	25	,	,	PUNCT
eurjchem-479	95	26	1h	1h	NUM
eurjchem-479	95	27	,	,	PUNCT
eurjchem-479	95	28	nh	nh	PROPN
eurjchem-479	95	29	)	)	PUNCT
eurjchem-479	95	30	,	,	PUNCT
eurjchem-479	95	31	11.47	11.47	NUM
eurjchem-479	95	32	(	(	PUNCT
eurjchem-479	95	33	s	s	PROPN
eurjchem-479	95	34	,	,	PUNCT
eurjchem-479	95	35	1h	1h	NUM
eurjchem-479	95	36	,	,	PUNCT
eurjchem-479	95	37	nh	nh	PROPN
eurjchem-479	95	38	)	)	PUNCT
eurjchem-479	95	39	.	.	PUNCT
eurjchem-479	96	1	anal	anal	PROPN
eurjchem-479	96	2	.	.	PUNCT
eurjchem-479	96	3	calcd	calcd	NOUN
eurjchem-479	96	4	.	.	PUNCT
eurjchem-479	97	1	for	for	ADP
eurjchem-479	97	2	c15h6brcl4n3o3	c15h6brcl4n3o3	NOUN
eurjchem-479	97	3	:	:	PUNCT
eurjchem-479	97	4	c	c	X
eurjchem-479	97	5	,	,	PUNCT
eurjchem-479	97	6	36.18	36.18	NUM
eurjchem-479	97	7	;	;	PUNCT
eurjchem-479	97	8	h	h	NOUN
eurjchem-479	97	9	,	,	PUNCT
eurjchem-479	97	10	1.21	1.21	NUM
eurjchem-479	97	11	;	;	PUNCT
eurjchem-479	97	12	n	n	CCONJ
eurjchem-479	97	13	,	,	PUNCT
eurjchem-479	97	14	8.44	8.44	NUM
eurjchem-479	97	15	.	.	PUNCT
eurjchem-479	98	1	found	find	VERB
eurjchem-479	98	2	:	:	PUNCT
eurjchem-479	99	1	c	c	X
eurjchem-479	99	2	,	,	PUNCT
eurjchem-479	99	3	36.28	36.28	NUM
eurjchem-479	99	4	;	;	PUNCT
eurjchem-479	99	5	h	h	NOUN
eurjchem-479	99	6	,	,	PUNCT
eurjchem-479	99	7	1.22	1.22	NUM
eurjchem-479	99	8	;	;	PUNCT
eurjchem-479	99	9	n	n	PRON
eurjchem-479	99	10	8.68	8.68	NUM
eurjchem-479	99	11	%	%	NOUN
eurjchem-479	99	12	.	.	PUNCT
eurjchem-479	100	1	2.2.9	2.2.9	X
eurjchem-479	100	2	.	.	PUNCT
eurjchem-479	101	1	3‐arylidineaminotetrachloroquinazolin‐2,4‐diones	3‐arylidineaminotetrachloroquinazolin‐2,4‐dione	NOUN
eurjchem-479	101	2	(	(	PUNCT
eurjchem-479	101	3	9a‐d	9a‐d	NOUN
eurjchem-479	101	4	)	)	PUNCT
eurjchem-479	101	5	3‐aminotetrachloroquinazolin‐2,4‐dione	3‐aminotetrachloroquinazolin‐2,4‐dione	NUM
eurjchem-479	101	6	3	3	NUM
eurjchem-479	101	7	(	(	PUNCT
eurjchem-479	101	8	0.31	0.31	NUM
eurjchem-479	101	9	g	g	NOUN
eurjchem-479	101	10	,	,	PUNCT
eurjchem-479	101	11	1	1	NUM
eurjchem-479	101	12	mmole	mmole	NOUN
eurjchem-479	101	13	)	)	PUNCT
eurjchem-479	101	14	was	be	AUX
eurjchem-479	101	15	heated	heat	VERB
eurjchem-479	101	16	under	under	ADP
eurjchem-479	101	17	reflux	reflux	NOUN
eurjchem-479	101	18	for	for	ADP
eurjchem-479	101	19	10‐12	10‐12	NUM
eurjchem-479	101	20	hours	hour	NOUN
eurjchem-479	101	21	with	with	ADP
eurjchem-479	101	22	the	the	DET
eurjchem-479	101	23	appropriate	appropriate	ADJ
eurjchem-479	101	24	aromatic	aromatic	ADJ
eurjchem-479	101	25	aldehydes	aldehyde	NOUN
eurjchem-479	101	26	namely	namely	ADV
eurjchem-479	101	27	benzaldehyde	benzaldehyde	NOUN
eurjchem-479	101	28	,	,	PUNCT
eurjchem-479	101	29	p‐nitrobenzaldehyde	p‐nitrobenzaldehyde	NOUN
eurjchem-479	101	30	,	,	PUNCT
eurjchem-479	101	31	p‐chlorobenzaldehyde	p‐chlorobenzaldehyde	PUNCT
eurjchem-479	101	32	and	and	CCONJ
eurjchem-479	101	33	thiophenecarbaldehyde	thiophenecarbaldehyde	NOUN
eurjchem-479	101	34	(	(	PUNCT
eurjchem-479	101	35	1	1	NUM
eurjchem-479	101	36	mmole	mmole	NOUN
eurjchem-479	101	37	)	)	PUNCT
eurjchem-479	101	38	in	in	ADP
eurjchem-479	101	39	absolute	absolute	ADJ
eurjchem-479	101	40	ethanol	ethanol	NOUN
eurjchem-479	101	41	(	(	PUNCT
eurjchem-479	101	42	20	20	NUM
eurjchem-479	101	43	ml	ml	NOUN
eurjchem-479	101	44	)	)	PUNCT
eurjchem-479	101	45	and	and	CCONJ
eurjchem-479	101	46	in	in	ADP
eurjchem-479	101	47	prescence	prescence	NOUN
eurjchem-479	101	48	of	of	ADP
eurjchem-479	101	49	pipridine	pipridine	NOUN
eurjchem-479	101	50	as	as	ADP
eurjchem-479	101	51	a	a	DET
eurjchem-479	101	52	catalyst	catalyst	NOUN
eurjchem-479	101	53	.	.	PUNCT
eurjchem-479	102	1	after	after	ADP
eurjchem-479	102	2	cooling	cool	VERB
eurjchem-479	102	3	;	;	PUNCT
eurjchem-479	102	4	the	the	DET
eurjchem-479	102	5	reaction	reaction	NOUN
eurjchem-479	102	6	mixture	mixture	NOUN
eurjchem-479	102	7	was	be	AUX
eurjchem-479	102	8	filtered	filter	VERB
eurjchem-479	102	9	off	off	ADP
eurjchem-479	102	10	and	and	CCONJ
eurjchem-479	102	11	crystallized	crystallize	VERB
eurjchem-479	102	12	from	from	ADP
eurjchem-479	102	13	appropriate	appropriate	ADJ
eurjchem-479	102	14	solvent	solvent	NOUN
eurjchem-479	102	15	to	to	PART
eurjchem-479	102	16	give	give	VERB
eurjchem-479	102	17	the	the	DET
eurjchem-479	102	18	arylidine	arylidine	NOUN
eurjchem-479	102	19	derivatives	derivative	NOUN
eurjchem-479	102	20	,	,	PUNCT
eurjchem-479	102	21	9a‐d	9a‐d	NOUN
eurjchem-479	102	22	,	,	PUNCT
eurjchem-479	102	23	respectively	respectively	ADV
eurjchem-479	102	24	(	(	PUNCT
eurjchem-479	102	25	scheme	scheme	NOUN
eurjchem-479	102	26	4	4	NUM
eurjchem-479	102	27	)	)	PUNCT
eurjchem-479	102	28	.	.	PUNCT
eurjchem-479	103	1	3‐(benzylidene‐amino)‐5,6,7,8‐tetrachloro‐1h‐quinazoline‐	3‐(benzylidene‐amino)‐5,6,7,8‐tetrachloro‐1h‐quinazoline‐	NUM
eurjchem-479	103	2	2,4‐dione	2,4‐dione	NUM
eurjchem-479	103	3	(	(	PUNCT
eurjchem-479	103	4	9a	9a	NOUN
eurjchem-479	103	5	):	):	PUNCT
eurjchem-479	103	6	yield	yield	NOUN
eurjchem-479	103	7	:	:	PUNCT
eurjchem-479	103	8	77	77	NUM
eurjchem-479	103	9	%	%	NOUN
eurjchem-479	103	10	as	as	ADP
eurjchem-479	103	11	yellow	yellow	ADJ
eurjchem-479	103	12	crystal	crystal	NOUN
eurjchem-479	103	13	.	.	PUNCT
eurjchem-479	104	1	m.p	m.p	PROPN
eurjchem-479	104	2	.	.	PROPN
eurjchem-479	104	3	:	:	PUNCT
eurjchem-479	105	1	360	360	NUM
eurjchem-479	105	2	oc	oc	NOUN
eurjchem-479	105	3	.	.	PUNCT
eurjchem-479	105	4	ft‐ir	ft‐ir	NOUN
eurjchem-479	105	5	(	(	PUNCT
eurjchem-479	105	6	kbr	kbr	PROPN
eurjchem-479	105	7	,	,	PUNCT
eurjchem-479	105	8	cm‐1	cm‐1	PROPN
eurjchem-479	105	9	):	):	PUNCT
eurjchem-479	105	10	3221	3221	NUM
eurjchem-479	105	11	(	(	PUNCT
eurjchem-479	105	12	nh	nh	NOUN
eurjchem-479	105	13	)	)	PUNCT
eurjchem-479	105	14	,	,	PUNCT
eurjchem-479	105	15	1731,1685	1731,1685	NUM
eurjchem-479	105	16	(	(	PUNCT
eurjchem-479	105	17	c	c	NOUN
eurjchem-479	105	18	=	=	NOUN
eurjchem-479	105	19	o	o	NOUN
eurjchem-479	105	20	)	)	PUNCT
eurjchem-479	105	21	.	.	PUNCT
eurjchem-479	106	1	1h	1h	NUM
eurjchem-479	106	2	nmr	nmr	NOUN
eurjchem-479	106	3	(	(	PUNCT
eurjchem-479	106	4	200	200	NUM
eurjchem-479	106	5	mhz	mhz	NOUN
eurjchem-479	106	6	,	,	PUNCT
eurjchem-479	106	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-479	106	8	,	,	PUNCT
eurjchem-479	106	9	ppm	ppm	NOUN
eurjchem-479	106	10	):	):	PUNCT
eurjchem-479	106	11	7.54‐7.95	7.54‐7.95	PROPN
eurjchem-479	106	12	(	(	PUNCT
eurjchem-479	106	13	m	m	PROPN
eurjchem-479	106	14	,	,	PUNCT
eurjchem-479	106	15	5h	5h	NUM
eurjchem-479	106	16	,	,	PUNCT
eurjchem-479	106	17	arom	arom	NOUN
eurjchem-479	106	18	.	.	PUNCT
eurjchem-479	107	1	h	h	X
eurjchem-479	107	2	)	)	PUNCT
eurjchem-479	107	3	,	,	PUNCT
eurjchem-479	107	4	8.6	8.6	NUM
eurjchem-479	107	5	(	(	PUNCT
eurjchem-479	107	6	s	s	PROPN
eurjchem-479	107	7	,	,	PUNCT
eurjchem-479	107	8	1h	1h	NUM
eurjchem-479	107	9	,	,	PUNCT
eurjchem-479	107	10	ch	ch	NOUN
eurjchem-479	107	11	=	=	NOUN
eurjchem-479	107	12	n	n	CCONJ
eurjchem-479	107	13	)	)	PUNCT
eurjchem-479	107	14	,	,	PUNCT
eurjchem-479	107	15	11.45	11.45	NUM
eurjchem-479	107	16	(	(	PUNCT
eurjchem-479	107	17	s	s	PROPN
eurjchem-479	107	18	,	,	PUNCT
eurjchem-479	107	19	1h	1h	NUM
eurjchem-479	107	20	,	,	PUNCT
eurjchem-479	107	21	nh	nh	PROPN
eurjchem-479	107	22	)	)	PUNCT
eurjchem-479	107	23	.	.	PUNCT
eurjchem-479	108	1	anal	anal	PROPN
eurjchem-479	108	2	.	.	PUNCT
eurjchem-479	108	3	calcd	calcd	NOUN
eurjchem-479	108	4	.	.	PUNCT
eurjchem-479	109	1	for	for	ADP
eurjchem-479	109	2	c15h7cl4n3o2	c15h7cl4n3o2	NOUN
eurjchem-479	109	3	:	:	PUNCT
eurjchem-479	109	4	c	c	X
eurjchem-479	109	5	,	,	PUNCT
eurjchem-479	109	6	44.71	44.71	NUM
eurjchem-479	109	7	;	;	PUNCT
eurjchem-479	109	8	h	h	X
eurjchem-479	109	9	,	,	PUNCT
eurjchem-479	109	10	1.75	1.75	NUM
eurjchem-479	109	11	;	;	PUNCT
eurjchem-479	109	12	n	n	CCONJ
eurjchem-479	109	13	,	,	PUNCT
eurjchem-479	109	14	10.42	10.42	NUM
eurjchem-479	109	15	.	.	PUNCT
eurjchem-479	109	16	found	find	VERB
eurjchem-479	109	17	:	:	PUNCT
eurjchem-479	110	1	c	c	X
eurjchem-479	110	2	,	,	PUNCT
eurjchem-479	110	3	44.94	44.94	NUM
eurjchem-479	110	4	;	;	PUNCT
eurjchem-479	110	5	h	h	NOUN
eurjchem-479	110	6	,	,	PUNCT
eurjchem-479	110	7	1.76	1.76	NUM
eurjchem-479	110	8	;	;	PUNCT
eurjchem-479	110	9	n	n	DET
eurjchem-479	110	10	10.59	10.59	NUM
eurjchem-479	110	11	%	%	NOUN
eurjchem-479	110	12	.	.	PUNCT
eurjchem-479	111	1	3‐(nitrobenzylidene‐amino)‐5,6,7,8‐tetrachloro‐1h‐	3‐(nitrobenzylidene‐amino)‐5,6,7,8‐tetrachloro‐1h‐	NUM
eurjchem-479	111	2	quinazoline‐2,4‐dione	quinazoline‐2,4‐dione	NOUN
eurjchem-479	111	3	(	(	PUNCT
eurjchem-479	111	4	9b	9b	NUM
eurjchem-479	111	5	):	):	PUNCT
eurjchem-479	111	6	yield	yield	NOUN
eurjchem-479	111	7	:	:	PUNCT
eurjchem-479	111	8	64	64	NUM
eurjchem-479	111	9	%	%	NOUN
eurjchem-479	111	10	as	as	ADP
eurjchem-479	111	11	brown	brown	ADJ
eurjchem-479	111	12	silky	silky	NOUN
eurjchem-479	111	13	.	.	PUNCT
eurjchem-479	112	1	m.p	m.p	PROPN
eurjchem-479	112	2	.	.	PROPN
eurjchem-479	112	3	:	:	PUNCT
eurjchem-479	113	1	360	360	NUM
eurjchem-479	113	2	oc	oc	NOUN
eurjchem-479	113	3	.	.	PUNCT
eurjchem-479	113	4	ft‐ir	ft‐ir	NOUN
eurjchem-479	113	5	(	(	PUNCT
eurjchem-479	113	6	kbr	kbr	PROPN
eurjchem-479	113	7	,	,	PUNCT
eurjchem-479	113	8	cm‐1	cm‐1	PROPN
eurjchem-479	113	9	):	):	PUNCT
eurjchem-479	113	10	3389	3389	NUM
eurjchem-479	113	11	(	(	PUNCT
eurjchem-479	113	12	nh	nh	NOUN
eurjchem-479	113	13	)	)	PUNCT
eurjchem-479	113	14	,	,	PUNCT
eurjchem-479	113	15	1726	1726	NUM
eurjchem-479	113	16	,	,	PUNCT
eurjchem-479	113	17	1623	1623	NUM
eurjchem-479	113	18	(	(	PUNCT
eurjchem-479	113	19	c	c	NOUN
eurjchem-479	113	20	=	=	NOUN
eurjchem-479	113	21	o	o	NOUN
eurjchem-479	113	22	)	)	PUNCT
eurjchem-479	113	23	.	.	PUNCT
eurjchem-479	114	1	1h	1h	NUM
eurjchem-479	114	2	nmr	nmr	NOUN
eurjchem-479	114	3	(	(	PUNCT
eurjchem-479	114	4	200	200	NUM
eurjchem-479	114	5	mhz	mhz	NOUN
eurjchem-479	114	6	,	,	PUNCT
eurjchem-479	114	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-479	114	8	,	,	PUNCT
eurjchem-479	114	9	ppm	ppm	NUM
eurjchem-479	114	10	):	):	PUNCT
eurjchem-479	114	11	8.24‐8.42	8.24‐8.42	NUM
eurjchem-479	114	12	(	(	PUNCT
eurjchem-479	114	13	two	two	NUM
eurjchem-479	114	14	d	d	PROPN
eurjchem-479	114	15	,	,	PUNCT
eurjchem-479	114	16	4h	4h	NUM
eurjchem-479	114	17	,	,	PUNCT
eurjchem-479	114	18	a2b2	a2b2	PROPN
eurjchem-479	114	19	arom	arom	ADJ
eurjchem-479	114	20	.	.	PUNCT
eurjchem-479	114	21	)	)	PUNCT
eurjchem-479	114	22	,	,	PUNCT
eurjchem-479	114	23	8.93	8.93	NUM
eurjchem-479	114	24	(	(	PUNCT
eurjchem-479	114	25	s	s	PROPN
eurjchem-479	114	26	,	,	PUNCT
eurjchem-479	114	27	1h	1h	NUM
eurjchem-479	114	28	,	,	PUNCT
eurjchem-479	114	29	ch	ch	NOUN
eurjchem-479	114	30	=	=	NOUN
eurjchem-479	114	31	n	n	CCONJ
eurjchem-479	114	32	)	)	PUNCT
eurjchem-479	114	33	,	,	PUNCT
eurjchem-479	114	34	11.20	11.20	NUM
eurjchem-479	114	35	(	(	PUNCT
eurjchem-479	114	36	s	s	PROPN
eurjchem-479	114	37	,	,	PUNCT
eurjchem-479	114	38	1h	1h	NUM
eurjchem-479	114	39	,	,	PUNCT
eurjchem-479	114	40	nh	nh	PROPN
eurjchem-479	114	41	)	)	PUNCT
eurjchem-479	114	42	.	.	PUNCT
eurjchem-479	115	1	anal	anal	PROPN
eurjchem-479	115	2	.	.	PUNCT
eurjchem-479	115	3	calcd	calcd	NOUN
eurjchem-479	115	4	.	.	PUNCT
eurjchem-479	116	1	for	for	ADP
eurjchem-479	116	2	c15h7cl4n3o2	c15h7cl4n3o2	NOUN
eurjchem-479	116	3	:	:	PUNCT
eurjchem-479	116	4	c	c	X
eurjchem-479	116	5	,	,	PUNCT
eurjchem-479	116	6	40.22	40.22	NUM
eurjchem-479	116	7	;	;	PUNCT
eurjchem-479	116	8	h	h	NOUN
eurjchem-479	116	9	,	,	PUNCT
eurjchem-479	116	10	1.35	1.35	NUM
eurjchem-479	116	11	;	;	PUNCT
eurjchem-479	116	12	n	n	CCONJ
eurjchem-479	116	13	,	,	PUNCT
eurjchem-479	116	14	12.51	12.51	NUM
eurjchem-479	116	15	.	.	PUNCT
eurjchem-479	116	16	found	find	VERB
eurjchem-479	116	17	:	:	PUNCT
eurjchem-479	117	1	c	c	X
eurjchem-479	117	2	,	,	PUNCT
eurjchem-479	117	3	40.51	40.51	NUM
eurjchem-479	117	4	;	;	PUNCT
eurjchem-479	117	5	h	h	NOUN
eurjchem-479	117	6	,	,	PUNCT
eurjchem-479	117	7	1.36	1.36	NUM
eurjchem-479	117	8	;	;	PUNCT
eurjchem-479	117	9	n	n	PRON
eurjchem-479	117	10	12.65	12.65	NUM
eurjchem-479	117	11	%	%	NOUN
eurjchem-479	117	12	.	.	PUNCT
eurjchem-479	118	1	3‐(chlorobenzylidene‐amino)‐5,6,7,8‐tetrachloro‐1h‐	3‐(chlorobenzylidene‐amino)‐5,6,7,8‐tetrachloro‐1h‐	NUM
eurjchem-479	118	2	quinazoline‐2,4‐dione	quinazoline‐2,4‐dione	NOUN
eurjchem-479	118	3	(	(	PUNCT
eurjchem-479	118	4	9c	9c	NUM
eurjchem-479	118	5	):	):	PUNCT
eurjchem-479	118	6	yield	yield	NOUN
eurjchem-479	118	7	:	:	PUNCT
eurjchem-479	118	8	60	60	NUM
eurjchem-479	118	9	%	%	NOUN
eurjchem-479	118	10	as	as	ADP
eurjchem-479	118	11	yellow	yellow	ADJ
eurjchem-479	118	12	crystal	crystal	NOUN
eurjchem-479	118	13	.	.	PUNCT
eurjchem-479	119	1	m.p	m.p	PROPN
eurjchem-479	119	2	.	.	PROPN
eurjchem-479	119	3	:	:	PUNCT
eurjchem-479	120	1	272	272	NUM
eurjchem-479	120	2	oc	oc	NOUN
eurjchem-479	120	3	.	.	PROPN
eurjchem-479	120	4	1h	1h	NUM
eurjchem-479	120	5	nmr	nmr	NOUN
eurjchem-479	120	6	(	(	PUNCT
eurjchem-479	120	7	200	200	NUM
eurjchem-479	120	8	mhz	mhz	NOUN
eurjchem-479	120	9	,	,	PUNCT
eurjchem-479	120	10	dmso‐d6	dmso‐d6	NOUN
eurjchem-479	120	11	,	,	PUNCT
eurjchem-479	120	12	ppm	ppm	NOUN
eurjchem-479	120	13	):	):	PUNCT
eurjchem-479	120	14	7.63‐7.90	7.63‐7.90	NUM
eurjchem-479	120	15	(	(	PUNCT
eurjchem-479	120	16	two	two	NUM
eurjchem-479	120	17	d	d	PROPN
eurjchem-479	120	18	,	,	PUNCT
eurjchem-479	120	19	4h	4h	NUM
eurjchem-479	120	20	,	,	PUNCT
eurjchem-479	120	21	a2b2	a2b2	PROPN
eurjchem-479	120	22	arom	arom	ADJ
eurjchem-479	120	23	.	.	PUNCT
eurjchem-479	120	24	)	)	PUNCT
eurjchem-479	120	25	,	,	PUNCT
eurjchem-479	120	26	8.79	8.79	NUM
eurjchem-479	120	27	(	(	PUNCT
eurjchem-479	120	28	s	s	PROPN
eurjchem-479	120	29	,	,	PUNCT
eurjchem-479	120	30	1h	1h	NUM
eurjchem-479	120	31	,	,	PUNCT
eurjchem-479	120	32	ch	ch	NOUN
eurjchem-479	120	33	=	=	NOUN
eurjchem-479	120	34	n	n	CCONJ
eurjchem-479	120	35	)	)	PUNCT
eurjchem-479	120	36	,	,	PUNCT
eurjchem-479	120	37	11.4	11.4	NUM
eurjchem-479	120	38	(	(	PUNCT
eurjchem-479	120	39	s	s	PROPN
eurjchem-479	120	40	,	,	PUNCT
eurjchem-479	120	41	1h	1h	NUM
eurjchem-479	120	42	,	,	PUNCT
eurjchem-479	120	43	nh	nh	PROPN
eurjchem-479	120	44	)	)	PUNCT
eurjchem-479	120	45	.	.	PUNCT
eurjchem-479	121	1	anal	anal	PROPN
eurjchem-479	121	2	.	.	PUNCT
eurjchem-479	121	3	calcd	calcd	NOUN
eurjchem-479	121	4	.	.	PUNCT
eurjchem-479	122	1	for	for	ADP
eurjchem-479	122	2	c15h6cl5n3o2	c15h6cl5n3o2	NOUN
eurjchem-479	122	3	:	:	PUNCT
eurjchem-479	122	4	c	c	X
eurjchem-479	122	5	,	,	PUNCT
eurjchem-479	122	6	41.19	41.19	NUM
eurjchem-479	122	7	;	;	PUNCT
eurjchem-479	122	8	h	h	NOUN
eurjchem-479	122	9	,	,	PUNCT
eurjchem-479	122	10	1.38	1.38	NUM
eurjchem-479	122	11	;	;	PUNCT
eurjchem-479	122	12	n	n	CCONJ
eurjchem-479	122	13	,	,	PUNCT
eurjchem-479	122	14	9.60	9.60	NUM
eurjchem-479	122	15	.	.	PUNCT
eurjchem-479	122	16	found	find	VERB
eurjchem-479	122	17	:	:	PUNCT
eurjchem-479	123	1	c	c	X
eurjchem-479	123	2	,	,	PUNCT
eurjchem-479	123	3	41.29	41.29	NUM
eurjchem-479	123	4	;	;	PUNCT
eurjchem-479	123	5	h	h	NOUN
eurjchem-479	123	6	,	,	PUNCT
eurjchem-479	123	7	1.39	1.39	NUM
eurjchem-479	123	8	;	;	PUNCT
eurjchem-479	123	9	n	n	PRON
eurjchem-479	123	10	9.89	9.89	NUM
eurjchem-479	123	11	%	%	NOUN
eurjchem-479	123	12	.	.	PUNCT
eurjchem-479	124	1	5,6,7,8‐tetrachloro‐3‐[(thiophen‐2‐ylmethylene)‐amino]‐1h‐	5,6,7,8‐tetrachloro‐3‐[(thiophen‐2‐ylmethylene)‐amino]‐1h‐	CCONJ
eurjchem-479	124	2	quinazoline‐2,4‐dione	quinazoline‐2,4‐dione	NOUN
eurjchem-479	124	3	(	(	PUNCT
eurjchem-479	124	4	9d	9d	NUM
eurjchem-479	124	5	):	):	PUNCT
eurjchem-479	124	6	yield	yield	NOUN
eurjchem-479	124	7	:	:	PUNCT
eurjchem-479	124	8	74	74	NUM
eurjchem-479	124	9	%	%	NOUN
eurjchem-479	124	10	as	as	ADP
eurjchem-479	124	11	yellow	yellow	ADJ
eurjchem-479	124	12	crystal	crystal	NOUN
eurjchem-479	124	13	.	.	PUNCT
eurjchem-479	125	1	m.p	m.p	PROPN
eurjchem-479	125	2	.	.	PROPN
eurjchem-479	125	3	:	:	PUNCT
eurjchem-479	125	4	320	320	NUM
eurjchem-479	125	5	oc	oc	NOUN
eurjchem-479	125	6	.	.	PUNCT
eurjchem-479	125	7	ft‐ir	ft‐ir	NOUN
eurjchem-479	125	8	(	(	PUNCT
eurjchem-479	125	9	kbr	kbr	PROPN
eurjchem-479	125	10	,	,	PUNCT
eurjchem-479	125	11	cm‐1	cm‐1	PROPN
eurjchem-479	125	12	):	):	PUNCT
eurjchem-479	125	13	3493	3493	NUM
eurjchem-479	125	14	(	(	PUNCT
eurjchem-479	125	15	nh	nh	NOUN
eurjchem-479	125	16	)	)	PUNCT
eurjchem-479	125	17	,	,	PUNCT
eurjchem-479	125	18	3108‐3032	3108‐3032	NUM
eurjchem-479	125	19	(	(	PUNCT
eurjchem-479	125	20	ch	ch	NOUN
eurjchem-479	125	21	aliph	aliph	PROPN
eurjchem-479	125	22	)	)	PUNCT
eurjchem-479	125	23	,	,	PUNCT
eurjchem-479	125	24	1751	1751	NUM
eurjchem-479	125	25	,	,	PUNCT
eurjchem-479	125	26	1695	1695	NUM
eurjchem-479	125	27	(	(	PUNCT
eurjchem-479	125	28	c	c	NOUN
eurjchem-479	125	29	=	=	NOUN
eurjchem-479	125	30	o	o	NOUN
eurjchem-479	125	31	)	)	PUNCT
eurjchem-479	125	32	.	.	PUNCT
eurjchem-479	126	1	1h	1h	NUM
eurjchem-479	126	2	nmr	nmr	NOUN
eurjchem-479	126	3	(	(	PUNCT
eurjchem-479	126	4	200	200	NUM
eurjchem-479	126	5	mhz	mhz	NOUN
eurjchem-479	126	6	,	,	PUNCT
eurjchem-479	126	7	dmso‐d6	dmso‐d6	NUM
eurjchem-479	126	8	):	):	PUNCT
eurjchem-479	126	9	7.30	7.30	NUM
eurjchem-479	126	10	(	(	PUNCT
eurjchem-479	126	11	dd	dd	PROPN
eurjchem-479	126	12	,	,	PUNCT
eurjchem-479	126	13	1h	1h	NUM
eurjchem-479	126	14	,	,	PUNCT
eurjchem-479	126	15	hx	hx	PROPN
eurjchem-479	126	16	)	)	PUNCT
eurjchem-479	126	17	,	,	PUNCT
eurjchem-479	126	18	7.78	7.78	NUM
eurjchem-479	126	19	(	(	PUNCT
eurjchem-479	126	20	dd	dd	PROPN
eurjchem-479	126	21	,	,	PUNCT
eurjchem-479	126	22	1h	1h	NUM
eurjchem-479	126	23	,	,	PUNCT
eurjchem-479	126	24	hm	hm	INTJ
eurjchem-479	126	25	)	)	PUNCT
eurjchem-479	126	26	,	,	PUNCT
eurjchem-479	126	27	7.96	7.96	NUM
eurjchem-479	126	28	(	(	PUNCT
eurjchem-479	126	29	dd	dd	PROPN
eurjchem-479	126	30	,	,	PUNCT
eurjchem-479	126	31	1h	1h	NUM
eurjchem-479	126	32	,	,	PUNCT
eurjchem-479	126	33	ha	ha	INTJ
eurjchem-479	126	34	)	)	PUNCT
eurjchem-479	126	35	,	,	PUNCT
eurjchem-479	126	36	8.8	8.8	NUM
eurjchem-479	126	37	(	(	PUNCT
eurjchem-479	126	38	s	s	PROPN
eurjchem-479	126	39	,	,	PUNCT
eurjchem-479	126	40	1h	1h	NUM
eurjchem-479	126	41	,	,	PUNCT
eurjchem-479	126	42	ch	ch	NOUN
eurjchem-479	126	43	=	=	NOUN
eurjchem-479	126	44	n	n	CCONJ
eurjchem-479	126	45	)	)	PUNCT
eurjchem-479	126	46	,	,	PUNCT
eurjchem-479	126	47	11.22	11.22	NUM
eurjchem-479	126	48	(	(	PUNCT
eurjchem-479	126	49	s	s	PROPN
eurjchem-479	126	50	,	,	PUNCT
eurjchem-479	126	51	1h	1h	NUM
eurjchem-479	126	52	,	,	PUNCT
eurjchem-479	126	53	nh	nh	PROPN
eurjchem-479	126	54	)	)	PUNCT
eurjchem-479	126	55	.	.	PUNCT
eurjchem-479	127	1	anal	anal	PROPN
eurjchem-479	127	2	.	.	PUNCT
eurjchem-479	127	3	calcd	calcd	NOUN
eurjchem-479	127	4	.	.	PUNCT
eurjchem-479	128	1	for	for	ADP
eurjchem-479	128	2	c13h5cl4n3o2s	c13h5cl4n3o2s	NOUN
eurjchem-479	128	3	:	:	PUNCT
eurjchem-479	128	4	c	c	X
eurjchem-479	128	5	,	,	PUNCT
eurjchem-479	128	6	38.17	38.17	NUM
eurjchem-479	128	7	;	;	PUNCT
eurjchem-479	128	8	h	h	NOUN
eurjchem-479	128	9	,	,	PUNCT
eurjchem-479	128	10	1.23	1.23	NUM
eurjchem-479	128	11	;	;	PUNCT
eurjchem-479	128	12	n	n	CCONJ
eurjchem-479	128	13	,	,	PUNCT
eurjchem-479	128	14	10.27	10.27	NUM
eurjchem-479	128	15	.	.	PUNCT
eurjchem-479	128	16	found	find	VERB
eurjchem-479	128	17	:	:	PUNCT
eurjchem-479	129	1	c	c	X
eurjchem-479	129	2	,	,	PUNCT
eurjchem-479	129	3	38.38	38.38	NUM
eurjchem-479	129	4	;	;	PUNCT
eurjchem-479	129	5	h	h	NOUN
eurjchem-479	129	6	,	,	PUNCT
eurjchem-479	129	7	1.24	1.24	NUM
eurjchem-479	129	8	;	;	PUNCT
eurjchem-479	129	9	n	n	DET
eurjchem-479	129	10	10.51	10.51	NUM
eurjchem-479	129	11	%	%	NOUN
eurjchem-479	129	12	.	.	PUNCT
eurjchem-479	130	1	2.2.10	2.2.10	NUM
eurjchem-479	130	2	.	.	PUNCT
eurjchem-479	131	1	n‐(5,6,‐7,8‐tetrachloro‐2,4‐dioxo‐1,4‐dihydro‐2h‐	n‐(5,6,‐7,8‐tetrachloro‐2,4‐dioxo‐1,4‐dihydro‐2h‐	ADJ
eurjchem-479	131	2	quinazolin‐3‐yl)‐malonamic	quinazolin‐3‐yl)‐malonamic	ADJ
eurjchem-479	131	3	acid	acid	NOUN
eurjchem-479	131	4	ethyl	ethyl	PROPN
eurjchem-479	131	5	ester	ester	NOUN
eurjchem-479	131	6	(	(	PUNCT
eurjchem-479	131	7	10	10	NUM
eurjchem-479	131	8	)	)	PUNCT
eurjchem-479	131	9	a	a	DET
eurjchem-479	131	10	mixture	mixture	NOUN
eurjchem-479	131	11	of	of	ADP
eurjchem-479	131	12	3‐aminotetrachloroquinazolin‐2,4‐dione	3‐aminotetrachloroquinazolin‐2,4‐dione	NUM
eurjchem-479	131	13	3	3	NUM
eurjchem-479	131	14	(	(	PUNCT
eurjchem-479	131	15	0.31	0.31	NUM
eurjchem-479	131	16	g	g	NOUN
eurjchem-479	131	17	,	,	PUNCT
eurjchem-479	131	18	1	1	NUM
eurjchem-479	131	19	mmole	mmole	NOUN
eurjchem-479	131	20	)	)	PUNCT
eurjchem-479	131	21	and	and	CCONJ
eurjchem-479	131	22	diethylmalonate	diethylmalonate	PROPN
eurjchem-479	131	23	was	be	AUX
eurjchem-479	131	24	refluxed	refluxe	VERB
eurjchem-479	131	25	for	for	ADP
eurjchem-479	131	26	6	6	NUM
eurjchem-479	131	27	hours	hour	NOUN
eurjchem-479	131	28	.	.	PUNCT
eurjchem-479	132	1	after	after	ADP
eurjchem-479	132	2	cooling	cool	VERB
eurjchem-479	132	3	;	;	PUNCT
eurjchem-479	132	4	the	the	DET
eurjchem-479	132	5	reaction	reaction	NOUN
eurjchem-479	132	6	mixture	mixture	NOUN
eurjchem-479	132	7	was	be	AUX
eurjchem-479	132	8	filtered	filter	VERB
eurjchem-479	132	9	off	off	ADP
eurjchem-479	132	10	and	and	CCONJ
eurjchem-479	132	11	crystallized	crystallize	VERB
eurjchem-479	132	12	from	from	ADP
eurjchem-479	132	13	benzene	benzene	NOUN
eurjchem-479	132	14	/	/	SYM
eurjchem-479	132	15	ethanol	ethanol	NOUN
eurjchem-479	132	16	to	to	PART
eurjchem-479	132	17	give	give	VERB
eurjchem-479	132	18	n‐(5,6,7,8‐	n‐(5,6,7,8‐	ADJ
eurjchem-479	132	19	tetrachloro‐2,4‐dioxo‐1,4‐di‐hydro‐2h‐quinazolin‐3‐yl)malon‐	tetrachloro‐2,4‐dioxo‐1,4‐di‐hydro‐2h‐quinazolin‐3‐yl)malon‐	NUM
eurjchem-479	132	20	amic	amic	ADJ
eurjchem-479	132	21	acid	acid	PROPN
eurjchem-479	132	22	ethyl	ethyl	PROPN
eurjchem-479	132	23	ester	ester	NOUN
eurjchem-479	132	24	(	(	PUNCT
eurjchem-479	132	25	0.34	0.34	NUM
eurjchem-479	132	26	g	g	NOUN
eurjchem-479	132	27	,	,	PUNCT
eurjchem-479	132	28	0.75	0.75	NUM
eurjchem-479	132	29	mmole	mmole	NOUN
eurjchem-479	132	30	)	)	PUNCT
eurjchem-479	132	31	10	10	NUM
eurjchem-479	132	32	in	in	ADP
eurjchem-479	132	33	yield	yield	NOUN
eurjchem-479	132	34	78	78	NUM
eurjchem-479	132	35	%	%	NOUN
eurjchem-479	132	36	as	as	ADP
eurjchem-479	132	37	white	white	PROPN
eurjchem-479	132	38	crystal	crystal	NOUN
eurjchem-479	132	39	(	(	PUNCT
eurjchem-479	132	40	scheme	scheme	NOUN
eurjchem-479	132	41	4	4	NUM
eurjchem-479	132	42	)	)	PUNCT
eurjchem-479	132	43	.	.	PUNCT
eurjchem-479	133	1	m.p	m.p	PROPN
eurjchem-479	133	2	.	.	PROPN
eurjchem-479	133	3	:	:	PUNCT
eurjchem-479	133	4	310	310	NUM
eurjchem-479	133	5	oc	oc	NOUN
eurjchem-479	133	6	.	.	PUNCT
eurjchem-479	133	7	ft‐ir	ft‐ir	NOUN
eurjchem-479	133	8	(	(	PUNCT
eurjchem-479	133	9	kbr	kbr	PROPN
eurjchem-479	133	10	,	,	PUNCT
eurjchem-479	133	11	cm‐1	cm‐1	PROPN
eurjchem-479	133	12	):	):	PUNCT
eurjchem-479	133	13	3200	3200	NUM
eurjchem-479	133	14	(	(	PUNCT
eurjchem-479	133	15	nh	nh	NOUN
eurjchem-479	133	16	)	)	PUNCT
eurjchem-479	133	17	,	,	PUNCT
eurjchem-479	133	18	1740	1740	NUM
eurjchem-479	133	19	and	and	CCONJ
eurjchem-479	133	20	1660	1660	NUM
eurjchem-479	133	21	(	(	PUNCT
eurjchem-479	133	22	c	c	NOUN
eurjchem-479	133	23	=	=	NOUN
eurjchem-479	133	24	o	o	NOUN
eurjchem-479	133	25	)	)	PUNCT
eurjchem-479	133	26	.	.	PUNCT
eurjchem-479	134	1	1h	1h	NUM
eurjchem-479	134	2	nmr	nmr	NOUN
eurjchem-479	134	3	(	(	PUNCT
eurjchem-479	134	4	200	200	NUM
eurjchem-479	134	5	mhz	mhz	NOUN
eurjchem-479	134	6	,	,	PUNCT
eurjchem-479	134	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-479	134	8	,	,	PUNCT
eurjchem-479	134	9	ppm	ppm	NOUN
eurjchem-479	134	10	):	):	PUNCT
eurjchem-479	134	11	1.18	1.18	NUM
eurjchem-479	134	12	(	(	PUNCT
eurjchem-479	134	13	t	t	PROPN
eurjchem-479	134	14	,	,	PUNCT
eurjchem-479	134	15	3h	3h	NUM
eurjchem-479	134	16	,	,	PUNCT
eurjchem-479	134	17	ch3	ch3	PROPN
eurjchem-479	134	18	)	)	PUNCT
eurjchem-479	134	19	,	,	PUNCT
eurjchem-479	134	20	3.50	3.50	NUM
eurjchem-479	134	21	(	(	PUNCT
eurjchem-479	134	22	s	s	PROPN
eurjchem-479	134	23	,	,	PUNCT
eurjchem-479	134	24	2h	2h	NUM
eurjchem-479	134	25	,	,	PUNCT
eurjchem-479	134	26	ch2‐co	ch2‐co	PROPN
eurjchem-479	134	27	)	)	PUNCT
eurjchem-479	134	28	,	,	PUNCT
eurjchem-479	134	29	4.13	4.13	NUM
eurjchem-479	134	30	(	(	PUNCT
eurjchem-479	134	31	q	q	NOUN
eurjchem-479	134	32	,	,	PUNCT
eurjchem-479	134	33	2h	2h	NUM
eurjchem-479	134	34	,	,	PUNCT
eurjchem-479	134	35	ch2‐	ch2‐	NOUN
eurjchem-479	134	36	o	o	NOUN
eurjchem-479	134	37	)	)	PUNCT
eurjchem-479	134	38	,	,	PUNCT
eurjchem-479	134	39	10.90	10.90	NUM
eurjchem-479	134	40	(	(	PUNCT
eurjchem-479	134	41	s	s	PROPN
eurjchem-479	134	42	,	,	PUNCT
eurjchem-479	134	43	1h	1h	NUM
eurjchem-479	134	44	,	,	PUNCT
eurjchem-479	134	45	nh	nh	PROPN
eurjchem-479	134	46	)	)	PUNCT
eurjchem-479	134	47	,	,	PUNCT
eurjchem-479	134	48	11.44	11.44	NUM
eurjchem-479	134	49	(	(	PUNCT
eurjchem-479	134	50	s	s	PROPN
eurjchem-479	134	51	,	,	PUNCT
eurjchem-479	134	52	1h	1h	NUM
eurjchem-479	134	53	,	,	PUNCT
eurjchem-479	134	54	nh	nh	PROPN
eurjchem-479	134	55	)	)	PUNCT
eurjchem-479	134	56	.	.	PUNCT
eurjchem-479	135	1	anal	anal	PROPN
eurjchem-479	135	2	.	.	PUNCT
eurjchem-479	135	3	calcd	calcd	NOUN
eurjchem-479	135	4	.	.	PUNCT
eurjchem-479	136	1	for	for	ADP
eurjchem-479	136	2	c13h9cl4n3o5	c13h9cl4n3o5	PROPN
eurjchem-479	136	3	:	:	PUNCT
eurjchem-479	136	4	c	c	X
eurjchem-479	136	5	,	,	PUNCT
eurjchem-479	136	6	36.39	36.39	NUM
eurjchem-479	136	7	;	;	PUNCT
eurjchem-479	136	8	h	h	NOUN
eurjchem-479	136	9	,	,	PUNCT
eurjchem-479	136	10	2.11	2.11	NUM
eurjchem-479	136	11	;	;	PUNCT
eurjchem-479	136	12	n	n	CCONJ
eurjchem-479	136	13	,	,	PUNCT
eurjchem-479	136	14	9.79	9.79	NUM
eurjchem-479	136	15	.	.	PUNCT
eurjchem-479	136	16	found	find	VERB
eurjchem-479	136	17	:	:	PUNCT
eurjchem-479	137	1	c	c	X
eurjchem-479	137	2	,	,	PUNCT
eurjchem-479	137	3	36.69	36.69	NUM
eurjchem-479	137	4	;	;	PUNCT
eurjchem-479	137	5	h	h	NOUN
eurjchem-479	137	6	,	,	PUNCT
eurjchem-479	137	7	2.12	2.12	NUM
eurjchem-479	137	8	;	;	PUNCT
eurjchem-479	137	9	n	n	PRON
eurjchem-479	137	10	9.98	9.98	NUM
eurjchem-479	137	11	%	%	NOUN
eurjchem-479	137	12	.	.	PUNCT
eurjchem-479	138	1	2.2.11	2.2.11	NUM
eurjchem-479	138	2	.	.	X
eurjchem-479	139	1	3‐(ethoxymethylidineamino)tetrachloroquinazolin‐	3‐(ethoxymethylidineamino)tetrachloroquinazolin‐	NUM
eurjchem-479	139	2	2,4‐dione	2,4‐dione	NUM
eurjchem-479	139	3	(	(	PUNCT
eurjchem-479	139	4	11	11	NUM
eurjchem-479	139	5	)	)	PUNCT
eurjchem-479	139	6	triethylorthoformate	triethylorthoformate	NOUN
eurjchem-479	139	7	is	be	AUX
eurjchem-479	139	8	added	add	VERB
eurjchem-479	139	9	to	to	ADP
eurjchem-479	139	10	3‐aminotetrachloro	3‐aminotetrachloro	NUM
eurjchem-479	139	11	quinazolin‐2,4‐dione	quinazolin‐2,4‐dione	NUM
eurjchem-479	139	12	3	3	NUM
eurjchem-479	139	13	(	(	PUNCT
eurjchem-479	139	14	0.31	0.31	NUM
eurjchem-479	139	15	g	g	NOUN
eurjchem-479	139	16	,	,	PUNCT
eurjchem-479	139	17	1	1	NUM
eurjchem-479	139	18	mmole	mmole	NOUN
eurjchem-479	139	19	)	)	PUNCT
eurjchem-479	139	20	.	.	PUNCT
eurjchem-479	140	1	the	the	DET
eurjchem-479	140	2	mixture	mixture	NOUN
eurjchem-479	140	3	was	be	AUX
eurjchem-479	140	4	refluxed	refluxe	VERB
eurjchem-479	140	5	for	for	ADP
eurjchem-479	140	6	6	6	NUM
eurjchem-479	140	7	hours	hour	NOUN
eurjchem-479	140	8	,	,	PUNCT
eurjchem-479	140	9	and	and	CCONJ
eurjchem-479	140	10	then	then	ADV
eurjchem-479	140	11	allowed	allow	VERB
eurjchem-479	140	12	to	to	PART
eurjchem-479	140	13	stand	stand	VERB
eurjchem-479	140	14	overnight	overnight	ADV
eurjchem-479	140	15	.	.	PUNCT
eurjchem-479	141	1	the	the	DET
eurjchem-479	141	2	precipitated	precipitate	VERB
eurjchem-479	141	3	product	product	NOUN
eurjchem-479	141	4	was	be	AUX
eurjchem-479	141	5	collected	collect	VERB
eurjchem-479	141	6	and	and	CCONJ
eurjchem-479	141	7	crystallized	crystallize	VERB
eurjchem-479	141	8	from	from	ADP
eurjchem-479	141	9	benzene	benzene	NOUN
eurjchem-479	141	10	to	to	PART
eurjchem-479	141	11	give	give	VERB
eurjchem-479	141	12	3‐(ethoxymethylidineamino)tetrachloro	3‐(ethoxymethylidineamino)tetrachloro	NUM
eurjchem-479	141	13	quinazolin‐2,4‐dione	quinazolin‐2,4‐dione	NOUN
eurjchem-479	141	14	(	(	PUNCT
eurjchem-479	141	15	0.27	0.27	NUM
eurjchem-479	141	16	g	g	NOUN
eurjchem-479	141	17	,	,	PUNCT
eurjchem-479	141	18	0.72	0.72	NUM
eurjchem-479	141	19	mmole	mmole	NOUN
eurjchem-479	141	20	)	)	PUNCT
eurjchem-479	141	21	11	11	NUM
eurjchem-479	141	22	in	in	ADP
eurjchem-479	141	23	yield	yield	NOUN
eurjchem-479	141	24	72	72	NUM
eurjchem-479	141	25	%	%	NOUN
eurjchem-479	141	26	as	as	ADP
eurjchem-479	141	27	yellow	yellow	ADJ
eurjchem-479	141	28	crystal	crystal	NOUN
eurjchem-479	141	29	(	(	PUNCT
eurjchem-479	141	30	scheme	scheme	NOUN
eurjchem-479	141	31	4	4	NUM
eurjchem-479	141	32	)	)	PUNCT
eurjchem-479	141	33	.	.	PUNCT
eurjchem-479	142	1	m.p	m.p	PROPN
eurjchem-479	142	2	.	.	PROPN
eurjchem-479	142	3	:	:	PUNCT
eurjchem-479	142	4	182	182	NUM
eurjchem-479	142	5	oc	oc	NOUN
eurjchem-479	142	6	.	.	PUNCT
eurjchem-479	143	1	ft‐ir	ft‐ir	NOUN
eurjchem-479	143	2	(	(	PUNCT
eurjchem-479	143	3	kbr	kbr	PROPN
eurjchem-479	143	4	,	,	PUNCT
eurjchem-479	143	5	cm‐1	cm‐1	PROPN
eurjchem-479	143	6	):	):	PUNCT
eurjchem-479	143	7	3293	3293	NUM
eurjchem-479	143	8	(	(	PUNCT
eurjchem-479	143	9	nh	nh	NOUN
eurjchem-479	143	10	)	)	PUNCT
eurjchem-479	143	11	,	,	PUNCT
eurjchem-479	143	12	1741	1741	NUM
eurjchem-479	143	13	and	and	CCONJ
eurjchem-479	143	14	1660	1660	NUM
eurjchem-479	143	15	(	(	PUNCT
eurjchem-479	143	16	c	c	NOUN
eurjchem-479	143	17	=	=	NOUN
eurjchem-479	143	18	o	o	NOUN
eurjchem-479	143	19	)	)	PUNCT
eurjchem-479	143	20	.	.	PUNCT
eurjchem-479	144	1	1h	1h	NUM
eurjchem-479	144	2	nmr	nmr	NOUN
eurjchem-479	144	3	(	(	PUNCT
eurjchem-479	144	4	200	200	NUM
eurjchem-479	144	5	mhz	mhz	NOUN
eurjchem-479	144	6	,	,	PUNCT
eurjchem-479	144	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-479	144	8	,	,	PUNCT
eurjchem-479	144	9	ppm	ppm	NOUN
eurjchem-479	144	10	):	):	PUNCT
eurjchem-479	144	11	1.37	1.37	NUM
eurjchem-479	144	12	(	(	PUNCT
eurjchem-479	144	13	two	two	NUM
eurjchem-479	144	14	interfered	interfere	VERB
eurjchem-479	144	15	triplets	triplet	NOUN
eurjchem-479	144	16	for	for	ADP
eurjchem-479	144	17	the	the	DET
eurjchem-479	144	18	two	two	NUM
eurjchem-479	144	19	isomeric	isomeric	ADJ
eurjchem-479	144	20	ch3	ch3	PROPN
eurjchem-479	144	21	protons	proton	NOUN
eurjchem-479	144	22	)	)	PUNCT
eurjchem-479	144	23	,	,	PUNCT
eurjchem-479	144	24	4.39	4.39	NUM
eurjchem-479	144	25	two	two	NUM
eurjchem-479	144	26	quartets	quartet	NOUN
eurjchem-479	144	27	for	for	ADP
eurjchem-479	144	28	ch2	ch2	PROPN
eurjchem-479	144	29	(	(	PUNCT
eurjchem-479	144	30	z	z	NOUN
eurjchem-479	144	31	)	)	PUNCT
eurjchem-479	144	32	,	,	PUNCT
eurjchem-479	144	33	4.55	4.55	NUM
eurjchem-479	144	34	for	for	ADP
eurjchem-479	144	35	ch2	ch2	PROPN
eurjchem-479	144	36	(	(	PUNCT
eurjchem-479	144	37	e	e	NOUN
eurjchem-479	144	38	)	)	PUNCT
eurjchem-479	144	39	in	in	ADP
eurjchem-479	144	40	integration	integration	NOUN
eurjchem-479	144	41	ratio	ratio	NOUN
eurjchem-479	144	42	(	(	PUNCT
eurjchem-479	144	43	2:3	2:3	NUM
eurjchem-479	144	44	)	)	PUNCT
eurjchem-479	144	45	,	,	PUNCT
eurjchem-479	144	46	respectively	respectively	ADV
eurjchem-479	144	47	,	,	PUNCT
eurjchem-479	144	48	7.98	7.98	NUM
eurjchem-479	144	49	(	(	PUNCT
eurjchem-479	144	50	s	s	PROPN
eurjchem-479	144	51	,	,	PUNCT
eurjchem-479	144	52	1h	1h	NUM
eurjchem-479	144	53	,	,	PUNCT
eurjchem-479	144	54	ch	ch	NOUN
eurjchem-479	144	55	(	(	PUNCT
eurjchem-479	144	56	z	z	NOUN
eurjchem-479	144	57	)	)	PUNCT
eurjchem-479	144	58	)	)	PUNCT
eurjchem-479	144	59	,	,	PUNCT
eurjchem-479	144	60	8.20	8.20	NUM
eurjchem-479	144	61	(	(	PUNCT
eurjchem-479	144	62	s	s	PROPN
eurjchem-479	144	63	,	,	PUNCT
eurjchem-479	144	64	1h	1h	NUM
eurjchem-479	144	65	,	,	PUNCT
eurjchem-479	144	66	ch	ch	NOUN
eurjchem-479	144	67	(	(	PUNCT
eurjchem-479	144	68	e	e	NOUN
eurjchem-479	144	69	)	)	PUNCT
eurjchem-479	144	70	)	)	PUNCT
eurjchem-479	144	71	,	,	PUNCT
eurjchem-479	144	72	11.22	11.22	NUM
eurjchem-479	144	73	(	(	PUNCT
eurjchem-479	144	74	s	s	PROPN
eurjchem-479	144	75	,	,	PUNCT
eurjchem-479	144	76	1h	1h	NUM
eurjchem-479	144	77	,	,	PUNCT
eurjchem-479	144	78	nh	nh	PROPN
eurjchem-479	144	79	)	)	PUNCT
eurjchem-479	144	80	.	.	PUNCT
eurjchem-479	145	1	anal	anal	PROPN
eurjchem-479	145	2	.	.	PUNCT
eurjchem-479	145	3	calcd	calcd	NOUN
eurjchem-479	145	4	.	.	PUNCT
eurjchem-479	146	1	for	for	SCONJ
eurjchem-479	146	2	c11h7cl4n3o3	c11h7cl4n3o3	NOUN
eurjchem-479	146	3	:	:	PUNCT
eurjchem-479	146	4	c	c	X
eurjchem-479	146	5	,	,	PUNCT
eurjchem-479	146	6	35.61	35.61	NUM
eurjchem-479	146	7	;	;	PUNCT
eurjchem-479	146	8	h	h	NOUN
eurjchem-479	146	9	,	,	PUNCT
eurjchem-479	146	10	1.90	1.90	NUM
eurjchem-479	146	11	;	;	PUNCT
eurjchem-479	146	12	n	n	CCONJ
eurjchem-479	146	13	,	,	PUNCT
eurjchem-479	146	14	11.33	11.33	NUM
eurjchem-479	146	15	.	.	PUNCT
eurjchem-479	146	16	found	find	VERB
eurjchem-479	146	17	:	:	PUNCT
eurjchem-479	146	18	c	c	X
eurjchem-479	146	19	,	,	PUNCT
eurjchem-479	146	20	35.85	35.85	NUM
eurjchem-479	146	21	;	;	PUNCT
eurjchem-479	146	22	h	h	X
eurjchem-479	146	23	,	,	PUNCT
eurjchem-479	146	24	1.91	1.91	NUM
eurjchem-479	146	25	;	;	PUNCT
eurjchem-479	146	26	n	n	DET
eurjchem-479	146	27	11.52	11.52	NUM
eurjchem-479	146	28	%	%	NOUN
eurjchem-479	146	29	.	.	PUNCT
eurjchem-479	147	1	hassan	hassan	PROPN
eurjchem-479	147	2	et	et	PROPN
eurjchem-479	147	3	al	al	PROPN
eurjchem-479	147	4	.	.	PUNCT
eurjchem-479	147	5	/	/	SYM
eurjchem-479	147	6	european	european	PROPN
eurjchem-479	147	7	journal	journal	PROPN
eurjchem-479	147	8	of	of	ADP
eurjchem-479	147	9	chemistry	chemistry	NOUN
eurjchem-479	147	10	2	2	NUM
eurjchem-479	147	11	(	(	PUNCT
eurjchem-479	147	12	4	4	NUM
eurjchem-479	147	13	)	)	PUNCT
eurjchem-479	147	14	(	(	PUNCT
eurjchem-479	147	15	2011	2011	NUM
eurjchem-479	147	16	)	)	PUNCT
eurjchem-479	147	17	514‐518	514‐518	NOUN
eurjchem-479	148	1	517	517	NUM
eurjchem-479	148	2	scheme	scheme	NOUN
eurjchem-479	148	3	4	4	NUM
eurjchem-479	148	4	2.2.12	2.2.12	NUM
eurjchem-479	148	5	.	.	PUNCT
eurjchem-479	149	1	n‐phenylthiocarbamoyl‐n‐tetrachloroquinazolin‐2,4‐	n‐phenylthiocarbamoyl‐n‐tetrachloroquinazolin‐2,4‐	NOUN
eurjchem-479	149	2	dione‐n'‐pheny‐lthiourea	dione‐n'‐pheny‐lthiourea	PROPN
eurjchem-479	149	3	(	(	PUNCT
eurjchem-479	149	4	12	12	NUM
eurjchem-479	149	5	)	)	PUNCT
eurjchem-479	149	6	heating	heating	NOUN
eurjchem-479	149	7	of	of	ADP
eurjchem-479	149	8	3‐aminotetrachloroquinazolin‐2,4‐dione	3‐aminotetrachloroquinazolin‐2,4‐dione	NUM
eurjchem-479	149	9	3	3	NUM
eurjchem-479	149	10	(	(	PUNCT
eurjchem-479	149	11	0.31	0.31	NUM
eurjchem-479	149	12	g	g	NOUN
eurjchem-479	149	13	,	,	PUNCT
eurjchem-479	149	14	1	1	NUM
eurjchem-479	149	15	mmole	mmole	NOUN
eurjchem-479	149	16	)	)	PUNCT
eurjchem-479	149	17	with	with	ADP
eurjchem-479	149	18	phenylisothiocyanate	phenylisothiocyanate	NOUN
eurjchem-479	149	19	in	in	ADP
eurjchem-479	149	20	absolute	absolute	ADJ
eurjchem-479	149	21	ethanol	ethanol	NOUN
eurjchem-479	149	22	(	(	PUNCT
eurjchem-479	149	23	20	20	NUM
eurjchem-479	149	24	ml	ml	NOUN
eurjchem-479	149	25	)	)	PUNCT
eurjchem-479	149	26	under	under	ADP
eurjchem-479	149	27	reflux	reflux	NOUN
eurjchem-479	149	28	for	for	ADP
eurjchem-479	149	29	6	6	NUM
eurjchem-479	149	30	hours	hour	NOUN
eurjchem-479	149	31	gave	give	VERB
eurjchem-479	149	32	after	after	ADP
eurjchem-479	149	33	cooling	cool	VERB
eurjchem-479	149	34	a	a	DET
eurjchem-479	149	35	solid	solid	ADJ
eurjchem-479	149	36	product	product	NOUN
eurjchem-479	149	37	which	which	PRON
eurjchem-479	149	38	was	be	AUX
eurjchem-479	149	39	filtered	filter	VERB
eurjchem-479	149	40	off	off	ADP
eurjchem-479	149	41	and	and	CCONJ
eurjchem-479	149	42	crystallized	crystallize	VERB
eurjchem-479	149	43	from	from	ADP
eurjchem-479	149	44	benzene	benzene	NOUN
eurjchem-479	149	45	to	to	PART
eurjchem-479	149	46	give	give	VERB
eurjchem-479	149	47	n‐	n‐	NOUN
eurjchem-479	149	48	phenylthiocarbamoyl‐n‐tetrachloroquinazolin‐2,4‐dione‐n'‐	phenylthiocarbamoyl‐n‐tetrachloroquinazolin‐2,4‐dione‐n'‐	VERB
eurjchem-479	149	49	phenylthiourea	phenylthiourea	NOUN
eurjchem-479	149	50	(	(	PUNCT
eurjchem-479	149	51	0.37	0.37	NUM
eurjchem-479	149	52	g	g	NOUN
eurjchem-479	149	53	,	,	PUNCT
eurjchem-479	149	54	0.62	0.62	NUM
eurjchem-479	149	55	mmole	mmole	NOUN
eurjchem-479	149	56	)	)	PUNCT
eurjchem-479	149	57	12	12	NUM
eurjchem-479	149	58	in	in	ADP
eurjchem-479	149	59	yield	yield	NOUN
eurjchem-479	149	60	63	63	NUM
eurjchem-479	149	61	%	%	NOUN
eurjchem-479	149	62	as	as	ADP
eurjchem-479	149	63	white	white	PROPN
eurjchem-479	149	64	crystal	crystal	NOUN
eurjchem-479	149	65	(	(	PUNCT
eurjchem-479	149	66	scheme	scheme	NOUN
eurjchem-479	149	67	4	4	NUM
eurjchem-479	149	68	)	)	PUNCT
eurjchem-479	149	69	.	.	PUNCT
eurjchem-479	150	1	m.p	m.p	PROPN
eurjchem-479	150	2	.	.	PROPN
eurjchem-479	150	3	:	:	PUNCT
eurjchem-479	151	1	210	210	NUM
eurjchem-479	151	2	oc	oc	NOUN
eurjchem-479	151	3	.	.	PUNCT
eurjchem-479	151	4	ft‐ir	ft‐ir	NOUN
eurjchem-479	151	5	(	(	PUNCT
eurjchem-479	151	6	kbr	kbr	PROPN
eurjchem-479	151	7	,	,	PUNCT
eurjchem-479	151	8	cm‐1	cm‐1	PROPN
eurjchem-479	151	9	):	):	PUNCT
eurjchem-479	151	10	3231	3231	NUM
eurjchem-479	151	11	,	,	PUNCT
eurjchem-479	151	12	3185	3185	NUM
eurjchem-479	151	13	,	,	PUNCT
eurjchem-479	151	14	3129	3129	NUM
eurjchem-479	151	15	(	(	PUNCT
eurjchem-479	151	16	nh	nh	NOUN
eurjchem-479	151	17	)	)	PUNCT
eurjchem-479	151	18	,	,	PUNCT
eurjchem-479	151	19	1731	1731	NUM
eurjchem-479	151	20	and	and	CCONJ
eurjchem-479	151	21	1695	1695	NUM
eurjchem-479	151	22	(	(	PUNCT
eurjchem-479	151	23	c	c	X
eurjchem-479	151	24	=	=	NOUN
eurjchem-479	151	25	o).1h	o).1h	ADJ
eurjchem-479	151	26	nmr	nmr	NOUN
eurjchem-479	151	27	(	(	PUNCT
eurjchem-479	151	28	200	200	NUM
eurjchem-479	151	29	mhz	mhz	NOUN
eurjchem-479	151	30	,	,	PUNCT
eurjchem-479	151	31	dmso‐d6	dmso‐d6	NOUN
eurjchem-479	151	32	,	,	PUNCT
eurjchem-479	151	33	ppm	ppm	NUM
eurjchem-479	151	34	):	):	PUNCT
eurjchem-479	151	35	6.90‐7.57	6.90‐7.57	NUM
eurjchem-479	151	36	(	(	PUNCT
eurjchem-479	151	37	m	m	PROPN
eurjchem-479	151	38	,	,	PUNCT
eurjchem-479	151	39	10	10	NUM
eurjchem-479	151	40	h	h	NOUN
eurjchem-479	151	41	,	,	PUNCT
eurjchem-479	151	42	aromatic	aromatic	ADJ
eurjchem-479	151	43	)	)	PUNCT
eurjchem-479	151	44	,	,	PUNCT
eurjchem-479	151	45	9.80	9.80	NUM
eurjchem-479	151	46	(	(	PUNCT
eurjchem-479	151	47	s	s	PROPN
eurjchem-479	151	48	,	,	PUNCT
eurjchem-479	151	49	1h	1h	NUM
eurjchem-479	151	50	,	,	PUNCT
eurjchem-479	151	51	hn‐cs	hn‐cs	NUM
eurjchem-479	151	52	)	)	PUNCT
eurjchem-479	151	53	,	,	PUNCT
eurjchem-479	151	54	11.20	11.20	NUM
eurjchem-479	151	55	(	(	PUNCT
eurjchem-479	151	56	s	s	PROPN
eurjchem-479	151	57	,	,	PUNCT
eurjchem-479	151	58	1h	1h	NUM
eurjchem-479	151	59	,	,	PUNCT
eurjchem-479	151	60	quinazoline	quinazoline	NOUN
eurjchem-479	151	61	nh	nh	PROPN
eurjchem-479	151	62	)	)	PUNCT
eurjchem-479	151	63	.	.	PUNCT
eurjchem-479	152	1	anal	anal	PROPN
eurjchem-479	152	2	.	.	PUNCT
eurjchem-479	152	3	calcd	calcd	NOUN
eurjchem-479	152	4	.	.	PUNCT
eurjchem-479	153	1	for	for	SCONJ
eurjchem-479	153	2	c22h13cl4n5o2s2	c22h13cl4n5o2s2	PROPN
eurjchem-479	153	3	:	:	PUNCT
eurjchem-479	153	4	c	c	X
eurjchem-479	153	5	,	,	PUNCT
eurjchem-479	153	6	45.15	45.15	NUM
eurjchem-479	153	7	;	;	PUNCT
eurjchem-479	153	8	h	h	NOUN
eurjchem-479	153	9	,	,	PUNCT
eurjchem-479	153	10	2.24	2.24	NUM
eurjchem-479	153	11	;	;	PUNCT
eurjchem-479	153	12	n	n	CCONJ
eurjchem-479	153	13	,	,	PUNCT
eurjchem-479	153	14	11.96	11.96	NUM
eurjchem-479	153	15	.	.	PUNCT
eurjchem-479	153	16	found	find	VERB
eurjchem-479	153	17	:	:	PUNCT
eurjchem-479	154	1	c	c	X
eurjchem-479	154	2	,	,	PUNCT
eurjchem-479	154	3	45.41	45.41	NUM
eurjchem-479	154	4	;	;	PUNCT
eurjchem-479	154	5	h	h	X
eurjchem-479	154	6	,	,	PUNCT
eurjchem-479	154	7	2.25	2.25	NUM
eurjchem-479	154	8	;	;	PUNCT
eurjchem-479	154	9	n	n	PRON
eurjchem-479	154	10	12.15	12.15	NUM
eurjchem-479	154	11	%	%	NOUN
eurjchem-479	154	12	.	.	PUNCT
eurjchem-479	155	1	2.2.13	2.2.13	NUM
eurjchem-479	155	2	.	.	PUNCT
eurjchem-479	156	1	n‐phenyl‐n'‐[(1h,3h)‐5,6,7,8‐tetrachloroquinazolin‐	n‐phenyl‐n'‐[(1h,3h)‐5,6,7,8‐tetrachloroquinazolin‐	ADV
eurjchem-479	156	2	2,4‐dion‐3‐yl]urea	2,4‐dion‐3‐yl]urea	NUM
eurjchem-479	156	3	(	(	PUNCT
eurjchem-479	156	4	13	13	NUM
eurjchem-479	156	5	)	)	PUNCT
eurjchem-479	156	6	when	when	SCONJ
eurjchem-479	156	7	a	a	DET
eurjchem-479	156	8	mixture	mixture	NOUN
eurjchem-479	156	9	of	of	ADP
eurjchem-479	156	10	3‐aminotetrachloroquinazolin‐2,4‐dione	3‐aminotetrachloroquinazolin‐2,4‐dione	NUM
eurjchem-479	156	11	3	3	NUM
eurjchem-479	156	12	(	(	PUNCT
eurjchem-479	156	13	0.31	0.31	NUM
eurjchem-479	156	14	g	g	NOUN
eurjchem-479	156	15	,	,	PUNCT
eurjchem-479	156	16	1	1	NUM
eurjchem-479	156	17	mmole	mmole	NOUN
eurjchem-479	156	18	)	)	PUNCT
eurjchem-479	156	19	and	and	CCONJ
eurjchem-479	156	20	phenyl	phenyl	NOUN
eurjchem-479	156	21	thiocyanate	thiocyanate	NOUN
eurjchem-479	156	22	in	in	ADP
eurjchem-479	156	23	dry	dry	ADJ
eurjchem-479	156	24	pyridine	pyridine	NOUN
eurjchem-479	156	25	(	(	PUNCT
eurjchem-479	156	26	10	10	NUM
eurjchem-479	156	27	ml	ml	NOUN
eurjchem-479	156	28	)	)	PUNCT
eurjchem-479	156	29	was	be	AUX
eurjchem-479	156	30	refluxed	refluxe	VERB
eurjchem-479	156	31	for	for	ADP
eurjchem-479	156	32	10	10	NUM
eurjchem-479	156	33	hours	hour	NOUN
eurjchem-479	156	34	.	.	PUNCT
eurjchem-479	157	1	after	after	ADP
eurjchem-479	157	2	cooling	cool	VERB
eurjchem-479	157	3	;	;	PUNCT
eurjchem-479	157	4	the	the	DET
eurjchem-479	157	5	reaction	reaction	NOUN
eurjchem-479	157	6	mixture	mixture	NOUN
eurjchem-479	157	7	was	be	AUX
eurjchem-479	157	8	poured	pour	VERB
eurjchem-479	157	9	into	into	ADP
eurjchem-479	157	10	ice‐water	ice‐water	NOUN
eurjchem-479	157	11	and	and	CCONJ
eurjchem-479	157	12	the	the	DET
eurjchem-479	157	13	solid	solid	ADJ
eurjchem-479	157	14	formed	form	VERB
eurjchem-479	157	15	was	be	AUX
eurjchem-479	157	16	filtered	filter	VERB
eurjchem-479	157	17	off	off	ADP
eurjchem-479	157	18	and	and	CCONJ
eurjchem-479	157	19	crystallized	crystallize	VERB
eurjchem-479	157	20	from	from	ADP
eurjchem-479	157	21	benzene	benzene	NOUN
eurjchem-479	157	22	to	to	PART
eurjchem-479	157	23	give	give	VERB
eurjchem-479	157	24	n‐phenyl‐n'‐	n‐phenyl‐n'‐	PROPN
eurjchem-479	157	25	[	[	X
eurjchem-479	157	26	(	(	PUNCT
eurjchem-479	157	27	1h,3h)‐5,6,7,8‐tetrachloro‐quinazolin‐2,4‐dion‐3‐yl]urea	1h,3h)‐5,6,7,8‐tetrachloro‐quinazolin‐2,4‐dion‐3‐yl]urea	NUM
eurjchem-479	157	28	(	(	PUNCT
eurjchem-479	157	29	0.25	0.25	NUM
eurjchem-479	157	30	g	g	NOUN
eurjchem-479	157	31	,	,	PUNCT
eurjchem-479	157	32	0.57	0.57	NUM
eurjchem-479	157	33	mmole	mmole	NOUN
eurjchem-479	157	34	)	)	PUNCT
eurjchem-479	157	35	13	13	NUM
eurjchem-479	157	36	in	in	ADP
eurjchem-479	157	37	yield	yield	NOUN
eurjchem-479	157	38	57	57	NUM
eurjchem-479	157	39	%	%	NOUN
eurjchem-479	157	40	(	(	PUNCT
eurjchem-479	157	41	scheme	scheme	NOUN
eurjchem-479	157	42	4	4	NUM
eurjchem-479	157	43	)	)	PUNCT
eurjchem-479	157	44	.	.	PUNCT
eurjchem-479	158	1	m.p	m.p	PROPN
eurjchem-479	158	2	.	.	PROPN
eurjchem-479	158	3	:	:	PUNCT
eurjchem-479	158	4	194	194	NUM
eurjchem-479	158	5	oc	oc	NOUN
eurjchem-479	158	6	.	.	PUNCT
eurjchem-479	158	7	ft‐ir	ft‐ir	NOUN
eurjchem-479	158	8	(	(	PUNCT
eurjchem-479	158	9	kbr	kbr	PROPN
eurjchem-479	158	10	,	,	PUNCT
eurjchem-479	158	11	cm‐1	cm‐1	PROPN
eurjchem-479	158	12	):	):	PUNCT
eurjchem-479	158	13	3200	3200	NUM
eurjchem-479	158	14	(	(	PUNCT
eurjchem-479	158	15	nh	nh	NOUN
eurjchem-479	158	16	)	)	PUNCT
eurjchem-479	158	17	,	,	PUNCT
eurjchem-479	158	18	1740	1740	NUM
eurjchem-479	158	19	and	and	CCONJ
eurjchem-479	158	20	1660	1660	NUM
eurjchem-479	158	21	(	(	PUNCT
eurjchem-479	158	22	c	c	NOUN
eurjchem-479	158	23	=	=	NOUN
eurjchem-479	158	24	o).1h	o).1h	ADJ
eurjchem-479	158	25	nmr	nmr	NOUN
eurjchem-479	158	26	(	(	PUNCT
eurjchem-479	158	27	200	200	NUM
eurjchem-479	158	28	mhz	mhz	NOUN
eurjchem-479	158	29	,	,	PUNCT
eurjchem-479	158	30	dmso‐d6	dmso‐d6	NOUN
eurjchem-479	158	31	,	,	PUNCT
eurjchem-479	158	32	ppm	ppm	NUM
eurjchem-479	158	33	):	):	PUNCT
eurjchem-479	158	34	6.98‐7.50	6.98‐7.50	NUM
eurjchem-479	158	35	(	(	PUNCT
eurjchem-479	158	36	m	m	PROPN
eurjchem-479	158	37	,	,	PUNCT
eurjchem-479	158	38	5	5	NUM
eurjchem-479	158	39	h	h	NOUN
eurjchem-479	158	40	,	,	PUNCT
eurjchem-479	158	41	aromatic	aromatic	ADJ
eurjchem-479	158	42	)	)	PUNCT
eurjchem-479	158	43	,	,	PUNCT
eurjchem-479	158	44	8.70	8.70	NUM
eurjchem-479	158	45	(	(	PUNCT
eurjchem-479	158	46	s	s	PROPN
eurjchem-479	158	47	,	,	PUNCT
eurjchem-479	158	48	1h	1h	NUM
eurjchem-479	158	49	,	,	PUNCT
eurjchem-479	158	50	nh	nh	PROPN
eurjchem-479	158	51	)	)	PUNCT
eurjchem-479	158	52	,	,	PUNCT
eurjchem-479	158	53	10.90	10.90	NUM
eurjchem-479	158	54	(	(	PUNCT
eurjchem-479	158	55	s	s	PROPN
eurjchem-479	158	56	,	,	PUNCT
eurjchem-479	158	57	1h	1h	NUM
eurjchem-479	158	58	,	,	PUNCT
eurjchem-479	158	59	nh	nh	PROPN
eurjchem-479	158	60	)	)	PUNCT
eurjchem-479	158	61	,	,	PUNCT
eurjchem-479	158	62	11.80	11.80	NUM
eurjchem-479	158	63	(	(	PUNCT
eurjchem-479	158	64	s	s	PROPN
eurjchem-479	158	65	,	,	PUNCT
eurjchem-479	158	66	1h	1h	NUM
eurjchem-479	158	67	,	,	PUNCT
eurjchem-479	158	68	nh	nh	PROPN
eurjchem-479	158	69	)	)	PUNCT
eurjchem-479	158	70	.	.	PUNCT
eurjchem-479	159	1	anal	anal	PROPN
eurjchem-479	159	2	.	.	PUNCT
eurjchem-479	159	3	calcd	calcd	NOUN
eurjchem-479	159	4	.	.	PUNCT
eurjchem-479	160	1	for	for	ADP
eurjchem-479	160	2	c15h8cl4n4o3	c15h8cl4n4o3	NOUN
eurjchem-479	160	3	:	:	PUNCT
eurjchem-479	160	4	c	c	X
eurjchem-479	160	5	,	,	PUNCT
eurjchem-479	160	6	41.51	41.51	NUM
eurjchem-479	160	7	;	;	PUNCT
eurjchem-479	160	8	h	h	NOUN
eurjchem-479	160	9	,	,	PUNCT
eurjchem-479	160	10	1.85	1.85	NUM
eurjchem-479	160	11	;	;	PUNCT
eurjchem-479	160	12	n	n	CCONJ
eurjchem-479	160	13	,	,	PUNCT
eurjchem-479	160	14	12.91	12.91	NUM
eurjchem-479	160	15	.	.	PUNCT
eurjchem-479	160	16	found	find	VERB
eurjchem-479	160	17	:	:	PUNCT
eurjchem-479	161	1	c	c	X
eurjchem-479	161	2	,	,	PUNCT
eurjchem-479	161	3	41.78	41.78	NUM
eurjchem-479	161	4	;	;	PUNCT
eurjchem-479	161	5	h	h	NOUN
eurjchem-479	161	6	,	,	PUNCT
eurjchem-479	161	7	1.86	1.86	NUM
eurjchem-479	161	8	;	;	PUNCT
eurjchem-479	161	9	n	n	PRON
eurjchem-479	161	10	13.18	13.18	NUM
eurjchem-479	161	11	%	%	NOUN
eurjchem-479	161	12	.	.	PUNCT
eurjchem-479	162	1	2.2.14	2.2.14	X
eurjchem-479	162	2	.	.	PUNCT
eurjchem-479	162	3	antibacterial	antibacterial	ADJ
eurjchem-479	162	4	studies	study	NOUN
eurjchem-479	162	5	sallmonela	sallmonela	VERB
eurjchem-479	162	6	typhi	typhi	ADV
eurjchem-479	162	7	,	,	PUNCT
eurjchem-479	162	8	staphylococcus	staphylococcus	NOUN
eurjchem-479	162	9	aureus	aureus	NOUN
eurjchem-479	162	10	,	,	PUNCT
eurjchem-479	162	11	bacillus	bacillus	NOUN
eurjchem-479	162	12	cereus	cereus	NOUN
eurjchem-479	162	13	and	and	CCONJ
eurjchem-479	162	14	bacillus	bacillus	NOUN
eurjchem-479	162	15	subtilis	subtili	NOUN
eurjchem-479	162	16	were	be	AUX
eurjchem-479	162	17	obtained	obtain	VERB
eurjchem-479	162	18	from	from	ADP
eurjchem-479	162	19	the	the	DET
eurjchem-479	162	20	faculty	faculty	NOUN
eurjchem-479	162	21	of	of	ADP
eurjchem-479	162	22	veterinary	veterinary	ADJ
eurjchem-479	162	23	medicine	medicine	NOUN
eurjchem-479	162	24	,	,	PUNCT
eurjchem-479	162	25	pathology	pathology	NOUN
eurjchem-479	162	26	department	department	PROPN
eurjchem-479	162	27	,	,	PUNCT
eurjchem-479	162	28	qena	qena	PROPN
eurjchem-479	162	29	,	,	PUNCT
eurjchem-479	162	30	egypt	egypt	PROPN
eurjchem-479	162	31	.	.	PUNCT
eurjchem-479	163	1	all	all	DET
eurjchem-479	163	2	the	the	DET
eurjchem-479	163	3	bacteria	bacteria	NOUN
eurjchem-479	163	4	were	be	AUX
eurjchem-479	163	5	grown	grow	VERB
eurjchem-479	163	6	on	on	ADP
eurjchem-479	163	7	the	the	DET
eurjchem-479	163	8	desired	desire	VERB
eurjchem-479	163	9	media	medium	NOUN
eurjchem-479	163	10	until	until	SCONJ
eurjchem-479	163	11	the	the	DET
eurjchem-479	163	12	desired	desire	VERB
eurjchem-479	163	13	growth	growth	NOUN
eurjchem-479	163	14	was	be	AUX
eurjchem-479	163	15	obtained	obtain	VERB
eurjchem-479	163	16	.	.	PUNCT
eurjchem-479	163	17	disc	disc	NOUN
eurjchem-479	163	18	diffusion	diffusion	NOUN
eurjchem-479	163	19	test	test	NOUN
eurjchem-479	163	20	[	[	X
eurjchem-479	163	21	14	14	NUM
eurjchem-479	163	22	]	]	X
eurjchem-479	163	23	:	:	PUNCT
eurjchem-479	163	24	whatman	whatman	PROPN
eurjchem-479	163	25	paper	paper	NOUN
eurjchem-479	163	26	no	no	NOUN
eurjchem-479	163	27	.	.	NOUN
eurjchem-479	163	28	1	1	NUM
eurjchem-479	163	29	filter	filter	NOUN
eurjchem-479	163	30	paper	paper	NOUN
eurjchem-479	163	31	was	be	AUX
eurjchem-479	163	32	used	use	VERB
eurjchem-479	163	33	to	to	PART
eurjchem-479	163	34	make	make	VERB
eurjchem-479	163	35	sterile	sterile	ADJ
eurjchem-479	163	36	disc	disc	NOUN
eurjchem-479	163	37	in	in	ADP
eurjchem-479	163	38	order	order	NOUN
eurjchem-479	163	39	to	to	PART
eurjchem-479	163	40	screen	screen	VERB
eurjchem-479	163	41	for	for	ADP
eurjchem-479	163	42	the	the	DET
eurjchem-479	163	43	antibacterial	antibacterial	ADJ
eurjchem-479	163	44	activity	activity	NOUN
eurjchem-479	163	45	of	of	ADP
eurjchem-479	163	46	sallmonela	sallmonela	NOUN
eurjchem-479	163	47	typhi	typhi	VERB
eurjchem-479	163	48	,	,	PUNCT
eurjchem-479	163	49	staphylococcus	staphylococcus	NOUN
eurjchem-479	163	50	aureus	aureus	NOUN
eurjchem-479	163	51	,	,	PUNCT
eurjchem-479	163	52	bacillus	bacillus	NOUN
eurjchem-479	163	53	cereus	cereus	NOUN
eurjchem-479	163	54	and	and	CCONJ
eurjchem-479	163	55	bacillus	bacillus	NOUN
eurjchem-479	163	56	subtilis	subtili	NOUN
eurjchem-479	163	57	.	.	PUNCT
eurjchem-479	164	1	this	this	DET
eurjchem-479	164	2	filter	filter	NOUN
eurjchem-479	164	3	paper	paper	NOUN
eurjchem-479	164	4	was	be	AUX
eurjchem-479	164	5	punctured	puncture	VERB
eurjchem-479	164	6	to	to	ADP
eurjchem-479	164	7	the	the	DET
eurjchem-479	164	8	shape	shape	NOUN
eurjchem-479	164	9	of	of	ADP
eurjchem-479	164	10	commercial	commercial	ADJ
eurjchem-479	164	11	antibiotic	antibiotic	ADJ
eurjchem-479	164	12	disc	disc	NOUN
eurjchem-479	164	13	and	and	CCONJ
eurjchem-479	164	14	discs	disc	NOUN
eurjchem-479	164	15	were	be	AUX
eurjchem-479	164	16	autoclaved	autoclave	VERB
eurjchem-479	164	17	at	at	ADP
eurjchem-479	164	18	121	121	NUM
eurjchem-479	164	19	°	°	ADP
eurjchem-479	164	20	c	c	NOUN
eurjchem-479	164	21	for	for	ADP
eurjchem-479	164	22	15	15	NUM
eurjchem-479	164	23	min	min	NOUN
eurjchem-479	164	24	.	.	PUNCT
eurjchem-479	165	1	the	the	DET
eurjchem-479	165	2	suspension	suspension	NOUN
eurjchem-479	165	3	of	of	ADP
eurjchem-479	165	4	bacteria	bacteria	NOUN
eurjchem-479	165	5	culture	culture	NOUN
eurjchem-479	165	6	was	be	AUX
eurjchem-479	165	7	prepared	prepare	VERB
eurjchem-479	165	8	according	accord	VERB
eurjchem-479	165	9	to	to	ADP
eurjchem-479	165	10	the	the	DET
eurjchem-479	165	11	macfarland	macfarland	NOUN
eurjchem-479	165	12	standard	standard	NOUN
eurjchem-479	165	13	0.5	0.5	NUM
eurjchem-479	165	14	and	and	CCONJ
eurjchem-479	165	15	was	be	AUX
eurjchem-479	165	16	lawned	lawne	VERB
eurjchem-479	165	17	onto	onto	ADP
eurjchem-479	165	18	the	the	DET
eurjchem-479	165	19	mueiller	mueiller	NOUN
eurjchem-479	165	20	hinton	hinton	PROPN
eurjchem-479	165	21	agar	agar	NOUN
eurjchem-479	165	22	plates	plate	NOUN
eurjchem-479	165	23	to	to	PART
eurjchem-479	165	24	produce	produce	VERB
eurjchem-479	165	25	the	the	DET
eurjchem-479	165	26	bacteria	bacteria	NOUN
eurjchem-479	165	27	field	field	NOUN
eurjchem-479	165	28	.	.	PUNCT
eurjchem-479	166	1	a	a	DET
eurjchem-479	166	2	sterile	sterile	NOUN
eurjchem-479	166	3	of	of	ADP
eurjchem-479	166	4	punctured	punctured	ADJ
eurjchem-479	166	5	filter	filter	NOUN
eurjchem-479	166	6	papers	paper	NOUN
eurjchem-479	166	7	was	be	AUX
eurjchem-479	166	8	placed	place	VERB
eurjchem-479	166	9	on	on	ADP
eurjchem-479	166	10	the	the	DET
eurjchem-479	166	11	bacteria	bacteria	NOUN
eurjchem-479	166	12	field	field	NOUN
eurjchem-479	166	13	by	by	ADP
eurjchem-479	166	14	sterile	sterile	ADJ
eurjchem-479	166	15	forceps	forceps	NOUN
eurjchem-479	166	16	and	and	CCONJ
eurjchem-479	166	17	the	the	DET
eurjchem-479	166	18	solubilized	solubilize	VERB
eurjchem-479	166	19	extract	extract	NOUN
eurjchem-479	166	20	then	then	ADV
eurjchem-479	166	21	was	be	AUX
eurjchem-479	166	22	pipetted	pipette	VERB
eurjchem-479	166	23	out	out	ADP
eurjchem-479	166	24	onto	onto	ADP
eurjchem-479	166	25	the	the	DET
eurjchem-479	166	26	surface	surface	NOUN
eurjchem-479	166	27	of	of	ADP
eurjchem-479	166	28	filter	filter	NOUN
eurjchem-479	166	29	paper	paper	NOUN
eurjchem-479	166	30	on	on	ADP
eurjchem-479	166	31	the	the	DET
eurjchem-479	166	32	bacteria	bacteria	NOUN
eurjchem-479	166	33	field	field	NOUN
eurjchem-479	166	34	.	.	PUNCT
eurjchem-479	167	1	tetracycline	tetracycline	PROPN
eurjchem-479	167	2	and	and	CCONJ
eurjchem-479	167	3	dmf	dmf	PROPN
eurjchem-479	167	4	was	be	AUX
eurjchem-479	167	5	used	use	VERB
eurjchem-479	167	6	as	as	ADP
eurjchem-479	167	7	a	a	DET
eurjchem-479	167	8	positive	positive	ADJ
eurjchem-479	167	9	and	and	CCONJ
eurjchem-479	167	10	negative	negative	ADJ
eurjchem-479	167	11	control	control	NOUN
eurjchem-479	167	12	.	.	PUNCT
eurjchem-479	168	1	the	the	DET
eurjchem-479	168	2	concentration	concentration	NOUN
eurjchem-479	168	3	of	of	ADP
eurjchem-479	168	4	the	the	DET
eurjchem-479	168	5	compounds	compound	NOUN
eurjchem-479	168	6	tested	test	VERB
eurjchem-479	168	7	was	be	AUX
eurjchem-479	168	8	50	50	NUM
eurjchem-479	168	9	mg	mg	NUM
eurjchem-479	168	10	/	/	SYM
eurjchem-479	168	11	ml	ml	NOUN
eurjchem-479	168	12	.	.	PUNCT
eurjchem-479	169	1	finally	finally	ADV
eurjchem-479	169	2	,	,	PUNCT
eurjchem-479	169	3	the	the	DET
eurjchem-479	169	4	plate	plate	NOUN
eurjchem-479	169	5	was	be	AUX
eurjchem-479	169	6	incubated	incubate	VERB
eurjchem-479	169	7	at	at	ADP
eurjchem-479	169	8	37	37	NUM
eurjchem-479	169	9	°	°	ADP
eurjchem-479	169	10	c	c	NOUN
eurjchem-479	169	11	and	and	CCONJ
eurjchem-479	169	12	the	the	DET
eurjchem-479	169	13	zone	zone	NOUN
eurjchem-479	169	14	inhibition	inhibition	NOUN
eurjchem-479	169	15	is	be	AUX
eurjchem-479	169	16	observed	observe	VERB
eurjchem-479	169	17	after	after	ADP
eurjchem-479	169	18	24‐	24‐	NUM
eurjchem-479	169	19	48	48	NUM
eurjchem-479	169	20	h	h	NOUN
eurjchem-479	169	21	and	and	CCONJ
eurjchem-479	169	22	measured	measure	VERB
eurjchem-479	169	23	as	as	ADP
eurjchem-479	169	24	mm	mm	PROPN
eurjchem-479	169	25	.	.	PROPN
eurjchem-479	170	1	3	3	NUM
eurjchem-479	170	2	.	.	NOUN
eurjchem-479	170	3	results	result	NOUN
eurjchem-479	170	4	and	and	CCONJ
eurjchem-479	170	5	discussion	discussion	NOUN
eurjchem-479	170	6	3.1	3.1	NUM
eurjchem-479	170	7	.	.	PUNCT
eurjchem-479	171	1	synthesis	synthesis	NOUN
eurjchem-479	171	2	as	as	ADP
eurjchem-479	171	3	a	a	DET
eurjchem-479	171	4	part	part	NOUN
eurjchem-479	171	5	of	of	ADP
eurjchem-479	171	6	our	our	PRON
eurjchem-479	171	7	program	program	NOUN
eurjchem-479	171	8	aimed	aim	VERB
eurjchem-479	171	9	to	to	PART
eurjchem-479	171	10	synthesize	synthesize	VERB
eurjchem-479	171	11	new	new	ADJ
eurjchem-479	171	12	pyrimidine	pyrimidine	NOUN
eurjchem-479	171	13	derivatives	derivative	NOUN
eurjchem-479	171	14	as	as	ADP
eurjchem-479	171	15	potential	potential	ADJ
eurjchem-479	171	16	pharmaceuticals	pharmaceutical	NOUN
eurjchem-479	171	17	and/or	and/or	CCONJ
eurjchem-479	171	18	agrochemicals	agrochemical	NOUN
eurjchem-479	171	19	,	,	PUNCT
eurjchem-479	171	20	we	we	PRON
eurjchem-479	171	21	report	report	VERB
eurjchem-479	171	22	here	here	ADV
eurjchem-479	171	23	the	the	DET
eurjchem-479	171	24	synthesis	synthesis	NOUN
eurjchem-479	171	25	of	of	ADP
eurjchem-479	171	26	new	new	ADJ
eurjchem-479	171	27	tetrachloroheterocyclic	tetrachloroheterocyclic	NOUN
eurjchem-479	171	28	compounds	compound	NOUN
eurjchem-479	171	29	such	such	ADJ
eurjchem-479	171	30	as	as	ADP
eurjchem-479	171	31	tetrachloro	tetrachloro	PROPN
eurjchem-479	171	32	quinazolindione	quinazolindione	NOUN
eurjchem-479	171	33	derivatives	derivative	NOUN
eurjchem-479	171	34	.	.	PUNCT
eurjchem-479	172	1	treatment	treatment	NOUN
eurjchem-479	172	2	of	of	ADP
eurjchem-479	172	3	n‐hydroxytetra	n‐hydroxytetra	PUNCT
eurjchem-479	172	4	chlorophthalimide	chlorophthalimide	NOUN
eurjchem-479	172	5	with	with	ADP
eurjchem-479	172	6	benzenesulphonyl	benzenesulphonyl	ADJ
eurjchem-479	172	7	chloride	chloride	NOUN
eurjchem-479	172	8	gave	give	VERB
eurjchem-479	172	9	compound	compound	NOUN
eurjchem-479	172	10	2	2	NUM
eurjchem-479	172	11	,	,	PUNCT
eurjchem-479	172	12	which	which	PRON
eurjchem-479	172	13	identified	identify	VERB
eurjchem-479	172	14	as	as	ADP
eurjchem-479	172	15	n‐phenylsulphonyloxytetra‐	n‐phenylsulphonyloxytetra‐	DET
eurjchem-479	172	16	chlorophthalimide	chlorophthalimide	NOUN
eurjchem-479	172	17	(	(	PUNCT
eurjchem-479	172	18	scheme	scheme	NOUN
eurjchem-479	172	19	1	1	NUM
eurjchem-479	172	20	)	)	PUNCT
eurjchem-479	172	21	.	.	PUNCT
eurjchem-479	173	1	the	the	DET
eurjchem-479	173	2	main	main	ADJ
eurjchem-479	173	3	fragmentation	fragmentation	NOUN
eurjchem-479	173	4	routes	route	NOUN
eurjchem-479	173	5	for	for	ADP
eurjchem-479	173	6	compound	compound	NOUN
eurjchem-479	173	7	2	2	NUM
eurjchem-479	173	8	are	be	AUX
eurjchem-479	173	9	shown	show	VERB
eurjchem-479	173	10	in	in	ADP
eurjchem-479	173	11	scheme	scheme	NOUN
eurjchem-479	173	12	5	5	NUM
eurjchem-479	173	13	.	.	PUNCT
eurjchem-479	174	1	treatment	treatment	NOUN
eurjchem-479	174	2	of	of	ADP
eurjchem-479	174	3	n‐phenylsulphonyloxytetrachlorophthalimide	n‐phenylsulphonyloxytetrachlorophthalimide	ADV
eurjchem-479	174	4	2	2	NUM
eurjchem-479	174	5	with	with	ADP
eurjchem-479	174	6	excess	excess	ADJ
eurjchem-479	174	7	hydrazine	hydrazine	NOUN
eurjchem-479	174	8	hydrate	hydrate	NOUN
eurjchem-479	174	9	in	in	ADP
eurjchem-479	174	10	dry	dry	ADJ
eurjchem-479	174	11	benzene	benzene	NOUN
eurjchem-479	174	12	afforded	afford	VERB
eurjchem-479	174	13	3‐	3‐	NUM
eurjchem-479	174	14	aminotetrachloroquinazolin‐2,4‐dione	aminotetrachloroquinazolin‐2,4‐dione	NOUN
eurjchem-479	174	15	,	,	PUNCT
eurjchem-479	174	16	3	3	NUM
eurjchem-479	174	17	(	(	PUNCT
eurjchem-479	174	18	scheme	scheme	NOUN
eurjchem-479	174	19	3	3	NUM
eurjchem-479	174	20	)	)	PUNCT
eurjchem-479	174	21	.	.	PUNCT
eurjchem-479	175	1	the	the	DET
eurjchem-479	175	2	reaction	reaction	NOUN
eurjchem-479	175	3	of	of	ADP
eurjchem-479	175	4	n‐phenylsulphonyloxytetrachlorophthalimide	n‐phenylsulphonyloxytetrachlorophthalimide	ADP
eurjchem-479	175	5	,	,	PUNCT
eurjchem-479	175	6	2	2	NUM
eurjchem-479	175	7	,	,	PUNCT
eurjchem-479	175	8	with	with	ADP
eurjchem-479	175	9	hydrazine	hydrazine	NOUN
eurjchem-479	175	10	may	may	AUX
eurjchem-479	175	11	proceed	proceed	VERB
eurjchem-479	175	12	according	accord	VERB
eurjchem-479	175	13	to	to	ADP
eurjchem-479	175	14	the	the	DET
eurjchem-479	175	15	following	follow	VERB
eurjchem-479	175	16	mechanism	mechanism	NOUN
eurjchem-479	175	17	(	(	PUNCT
eurjchem-479	175	18	scheme	scheme	NOUN
eurjchem-479	175	19	6	6	NUM
eurjchem-479	175	20	)	)	PUNCT
eurjchem-479	175	21	.	.	PUNCT
eurjchem-479	176	1	the	the	DET
eurjchem-479	176	2	reaction	reaction	NOUN
eurjchem-479	176	3	of	of	ADP
eurjchem-479	176	4	compound	compound	NOUN
eurjchem-479	176	5	3	3	NUM
eurjchem-479	176	6	with	with	ADP
eurjchem-479	176	7	different	different	ADJ
eurjchem-479	176	8	acid	acid	NOUN
eurjchem-479	176	9	chlorides	chloride	NOUN
eurjchem-479	176	10	was	be	AUX
eurjchem-479	176	11	intensively	intensively	ADV
eurjchem-479	176	12	investigated	investigate	VERB
eurjchem-479	176	13	.	.	PUNCT
eurjchem-479	177	1	several	several	ADJ
eurjchem-479	177	2	3‐substituted	3‐substituted	NUM
eurjchem-479	177	3	518	518	NUM
eurjchem-479	177	4	hassan	hassan	PROPN
eurjchem-479	177	5	et	et	PROPN
eurjchem-479	177	6	al	al	PROPN
eurjchem-479	177	7	.	.	PUNCT
eurjchem-479	177	8	/	/	SYM
eurjchem-479	177	9	european	european	PROPN
eurjchem-479	177	10	journal	journal	PROPN
eurjchem-479	177	11	of	of	ADP
eurjchem-479	177	12	chemistry	chemistry	NOUN
eurjchem-479	177	13	2	2	NUM
eurjchem-479	177	14	(	(	PUNCT
eurjchem-479	177	15	4	4	NUM
eurjchem-479	177	16	)	)	PUNCT
eurjchem-479	177	17	(	(	PUNCT
eurjchem-479	177	18	2011	2011	NUM
eurjchem-479	177	19	)	)	PUNCT
eurjchem-479	177	20	514‐518	514‐518	PROPN
eurjchem-479	177	21	tetrachloroquinazolin‐2,4‐diones	tetrachloroquinazolin‐2,4‐diones	PROPN
eurjchem-479	177	22	,	,	PUNCT
eurjchem-479	177	23	4	4	NUM
eurjchem-479	177	24	,	,	PUNCT
eurjchem-479	177	25	5	5	NUM
eurjchem-479	177	26	,	,	PUNCT
eurjchem-479	177	27	6	6	NUM
eurjchem-479	177	28	,	,	PUNCT
eurjchem-479	177	29	7	7	NUM
eurjchem-479	177	30	,	,	PUNCT
eurjchem-479	177	31	8a	8a	NUM
eurjchem-479	177	32	and	and	CCONJ
eurjchem-479	177	33	8b	8b	NUM
eurjchem-479	177	34	were	be	AUX
eurjchem-479	177	35	prepared	prepare	VERB
eurjchem-479	177	36	via	via	ADP
eurjchem-479	177	37	treatment	treatment	NOUN
eurjchem-479	177	38	of	of	ADP
eurjchem-479	177	39	3‐aminotetrachloroquinazolin‐2,4‐	3‐aminotetrachloroquinazolin‐2,4‐	NUM
eurjchem-479	177	40	dione	dione	NOUN
eurjchem-479	177	41	3	3	NUM
eurjchem-479	177	42	with	with	ADP
eurjchem-479	177	43	acid	acid	NOUN
eurjchem-479	177	44	chlorides	chloride	NOUN
eurjchem-479	177	45	namely	namely	ADV
eurjchem-479	177	46	acetylchloride	acetylchloride	ADV
eurjchem-479	177	47	,	,	PUNCT
eurjchem-479	177	48	benzene	benzene	NOUN
eurjchem-479	177	49	sulphonylchloride	sulphonylchloride	NOUN
eurjchem-479	177	50	,	,	PUNCT
eurjchem-479	177	51	2‐thiophenecarbonyl‐chloride	2‐thiophenecarbonyl‐chloride	NUM
eurjchem-479	177	52	,	,	PUNCT
eurjchem-479	177	53	chloroacetyl	chloroacetyl	NOUN
eurjchem-479	177	54	chloride	chloride	NOUN
eurjchem-479	177	55	,	,	PUNCT
eurjchem-479	177	56	benzoylchloride	benzoylchloride	NOUN
eurjchem-479	177	57	and	and	CCONJ
eurjchem-479	177	58	p‐bromobenzoylchloride	p‐bromobenzoylchloride	ADP
eurjchem-479	177	59	(	(	PUNCT
eurjchem-479	177	60	scheme	scheme	NOUN
eurjchem-479	177	61	3	3	NUM
eurjchem-479	177	62	)	)	PUNCT
eurjchem-479	177	63	.	.	PUNCT
eurjchem-479	178	1	the	the	DET
eurjchem-479	178	2	reactions	reaction	NOUN
eurjchem-479	178	3	of	of	ADP
eurjchem-479	178	4	compound	compound	NOUN
eurjchem-479	178	5	3	3	NUM
eurjchem-479	178	6	with	with	ADP
eurjchem-479	178	7	different	different	ADJ
eurjchem-479	178	8	aldehydes	aldehyde	NOUN
eurjchem-479	178	9	,	,	PUNCT
eurjchem-479	178	10	diethylmalonate	diethylmalonate	ADJ
eurjchem-479	178	11	,	,	PUNCT
eurjchem-479	178	12	triethylorthoformate	triethylorthoformate	ADJ
eurjchem-479	178	13	,	,	PUNCT
eurjchem-479	178	14	phenyl	phenyl	NOUN
eurjchem-479	178	15	isothiocyanate	isothiocyanate	NOUN
eurjchem-479	178	16	and	and	CCONJ
eurjchem-479	178	17	phenyl	phenyl	NOUN
eurjchem-479	178	18	thiocyanate	thiocyanate	NOUN
eurjchem-479	178	19	were	be	AUX
eurjchem-479	178	20	intensively	intensively	ADV
eurjchem-479	178	21	investigated	investigate	VERB
eurjchem-479	178	22	.	.	PUNCT
eurjchem-479	179	1	several	several	ADJ
eurjchem-479	179	2	3‐arylidineaminotetrachloroquinazolin‐2,4‐diones	3‐arylidineaminotetrachloroquinazolin‐2,4‐dione	NOUN
eurjchem-479	179	3	9a‐d	9a‐d	NOUN
eurjchem-479	179	4	have	have	AUX
eurjchem-479	179	5	been	be	AUX
eurjchem-479	179	6	prepared	prepare	VERB
eurjchem-479	179	7	via	via	ADP
eurjchem-479	179	8	treatment	treatment	NOUN
eurjchem-479	179	9	of	of	ADP
eurjchem-479	179	10	3‐aminotetrachloroquinazolin‐	3‐aminotetrachloroquinazolin‐	NUM
eurjchem-479	179	11	2,4‐dione	2,4‐dione	NUM
eurjchem-479	179	12	,	,	PUNCT
eurjchem-479	179	13	3	3	NUM
eurjchem-479	179	14	,	,	PUNCT
eurjchem-479	179	15	with	with	ADP
eurjchem-479	179	16	different	different	ADJ
eurjchem-479	179	17	aldehydes	aldehyde	NOUN
eurjchem-479	179	18	,	,	PUNCT
eurjchem-479	179	19	namely	namely	ADV
eurjchem-479	179	20	benzaldehyde	benzaldehyde	NOUN
eurjchem-479	179	21	,	,	PUNCT
eurjchem-479	179	22	p‐nitrobenzaldehyde	p‐nitrobenzaldehyde	NOUN
eurjchem-479	179	23	,	,	PUNCT
eurjchem-479	179	24	p‐chlorobenzaldehyde	p‐chlorobenzaldehyde	PUNCT
eurjchem-479	179	25	and	and	CCONJ
eurjchem-479	179	26	thiophene	thiophene	NOUN
eurjchem-479	179	27	carbaldehyde	carbaldehyde	NOUN
eurjchem-479	179	28	(	(	PUNCT
eurjchem-479	179	29	scheme	scheme	NOUN
eurjchem-479	179	30	4	4	NUM
eurjchem-479	179	31	)	)	PUNCT
eurjchem-479	179	32	.	.	PUNCT
eurjchem-479	180	1	also	also	ADV
eurjchem-479	180	2	,	,	PUNCT
eurjchem-479	180	3	3‐aminotetrachloroquinazolin‐	3‐aminotetrachloroquinazolin‐	NUM
eurjchem-479	180	4	2,4‐dione	2,4‐dione	NUM
eurjchem-479	180	5	,	,	PUNCT
eurjchem-479	180	6	3	3	NUM
eurjchem-479	180	7	,	,	PUNCT
eurjchem-479	180	8	reacted	react	VERB
eurjchem-479	180	9	with	with	ADP
eurjchem-479	180	10	diethylmalonate	diethylmalonate	ADJ
eurjchem-479	180	11	,	,	PUNCT
eurjchem-479	180	12	triethylortho‐	triethylortho‐	NOUN
eurjchem-479	180	13	formate	formate	NOUN
eurjchem-479	180	14	,	,	PUNCT
eurjchem-479	180	15	phenyl	phenyl	NOUN
eurjchem-479	180	16	isothiocyanate	isothiocyanate	NOUN
eurjchem-479	180	17	and	and	CCONJ
eurjchem-479	180	18	phenyl	phenyl	NOUN
eurjchem-479	180	19	thiocyanate	thiocyanate	NOUN
eurjchem-479	180	20	to	to	PART
eurjchem-479	180	21	give	give	VERB
eurjchem-479	180	22	n‐(5,6,‐7,8‐tetrachloro‐2,4‐dioxo‐1,4‐dihydro‐2h‐quinazolin‐3‐	n‐(5,6,‐7,8‐tetrachloro‐2,4‐dioxo‐1,4‐dihydro‐2h‐quinazolin‐3‐	NOUN
eurjchem-479	180	23	yl)‐malonamic	yl)‐malonamic	ADJ
eurjchem-479	180	24	acid	acid	PROPN
eurjchem-479	180	25	ethyl	ethyl	PROPN
eurjchem-479	180	26	ester	ester	NOUN
eurjchem-479	180	27	,	,	PUNCT
eurjchem-479	180	28	10	10	NUM
eurjchem-479	180	29	,	,	PUNCT
eurjchem-479	180	30	3‐(ethoxymethylidine‐	3‐(ethoxymethylidine‐	NUM
eurjchem-479	180	31	amino)tetrachloroquinazolin‐2,4‐dione	amino)tetrachloroquinazolin‐2,4‐dione	NOUN
eurjchem-479	180	32	,	,	PUNCT
eurjchem-479	180	33	11	11	NUM
eurjchem-479	180	34	,	,	PUNCT
eurjchem-479	180	35	n‐phenylthio	n‐phenylthio	PUNCT
eurjchem-479	180	36	carbamoyl‐n‐tetrachloroquinazolin‐2,4‐dione‐n'‐phenyl‐	carbamoyl‐n‐tetrachloroquinazolin‐2,4‐dione‐n'‐phenyl‐	NOUN
eurjchem-479	180	37	thiourea	thiourea	NOUN
eurjchem-479	180	38	,	,	PUNCT
eurjchem-479	180	39	12	12	NUM
eurjchem-479	180	40	,	,	PUNCT
eurjchem-479	180	41	and	and	CCONJ
eurjchem-479	180	42	n‐phenyl‐n'‐[(1h,3h)‐5,6,7,8‐tetrachloro	n‐phenyl‐n'‐[(1h,3h)‐5,6,7,8‐tetrachloro	PROPN
eurjchem-479	180	43	quinazolin‐2,4‐dion‐3‐yl]urea	quinazolin‐2,4‐dion‐3‐yl]urea	NOUN
eurjchem-479	180	44	,	,	PUNCT
eurjchem-479	180	45	13	13	NUM
eurjchem-479	180	46	,	,	PUNCT
eurjchem-479	180	47	respectively	respectively	ADV
eurjchem-479	180	48	(	(	PUNCT
eurjchem-479	180	49	scheme	scheme	NOUN
eurjchem-479	180	50	4	4	NUM
eurjchem-479	180	51	)	)	PUNCT
eurjchem-479	180	52	.	.	PUNCT
eurjchem-479	181	1	scheme	scheme	NOUN
eurjchem-479	181	2	5	5	NUM
eurjchem-479	181	3	3.2	3.2	NUM
eurjchem-479	181	4	.	.	PUNCT
eurjchem-479	182	1	antibacterial	antibacterial	ADJ
eurjchem-479	182	2	assays	assay	NOUN
eurjchem-479	182	3	the	the	DET
eurjchem-479	182	4	compound	compound	NOUN
eurjchem-479	182	5	3	3	NUM
eurjchem-479	182	6	exhibited	exhibit	VERB
eurjchem-479	182	7	anti‐bacterialactivity	anti‐bacterialactivity	NOUN
eurjchem-479	182	8	against	against	ADP
eurjchem-479	182	9	staph	staph	NOUN
eurjchem-479	182	10	.	.	PUNCT
eurjchem-479	183	1	areus	areus	NOUN
eurjchem-479	183	2	(	(	PUNCT
eurjchem-479	183	3	8	8	NUM
eurjchem-479	183	4	mm	mm	NOUN
eurjchem-479	183	5	)	)	PUNCT
eurjchem-479	183	6	,	,	PUNCT
eurjchem-479	183	7	bacillus	bacillus	NOUN
eurjchem-479	183	8	cereus	cereus	NOUN
eurjchem-479	183	9	(	(	PUNCT
eurjchem-479	183	10	15	15	NUM
eurjchem-479	183	11	mm	mm	NOUN
eurjchem-479	183	12	)	)	PUNCT
eurjchem-479	183	13	and	and	CCONJ
eurjchem-479	183	14	bacillus	bacillus	NOUN
eurjchem-479	183	15	subtilis	subtili	NOUN
eurjchem-479	183	16	(	(	PUNCT
eurjchem-479	183	17	9	9	NUM
eurjchem-479	183	18	mm	mm	NOUN
eurjchem-479	183	19	)	)	PUNCT
eurjchem-479	183	20	.	.	PUNCT
eurjchem-479	184	1	on	on	ADP
eurjchem-479	184	2	the	the	DET
eurjchem-479	184	3	other	other	ADJ
eurjchem-479	184	4	hand	hand	NOUN
eurjchem-479	184	5	this	this	DET
eurjchem-479	184	6	compound	compound	NOUN
eurjchem-479	184	7	did	do	AUX
eurjchem-479	184	8	n't	not	PART
eurjchem-479	184	9	show	show	VERB
eurjchem-479	184	10	any	any	DET
eurjchem-479	184	11	inhibition	inhibition	NOUN
eurjchem-479	184	12	activity	activity	NOUN
eurjchem-479	184	13	against	against	ADP
eurjchem-479	184	14	salmonella	salmonella	NOUN
eurjchem-479	184	15	typhi	typhi	ADV
eurjchem-479	184	16	.	.	PUNCT
eurjchem-479	185	1	this	this	PRON
eurjchem-479	185	2	may	may	AUX
eurjchem-479	185	3	be	be	AUX
eurjchem-479	185	4	due	due	ADJ
eurjchem-479	185	5	to	to	ADP
eurjchem-479	185	6	four	four	NUM
eurjchem-479	185	7	chlorine	chlorine	NOUN
eurjchem-479	185	8	[	[	X
eurjchem-479	185	9	15	15	NUM
eurjchem-479	185	10	]	]	PUNCT
eurjchem-479	185	11	atoms	atom	NOUN
eurjchem-479	185	12	and	and	CCONJ
eurjchem-479	185	13	pyrimidine	pyrimidine	NOUN
eurjchem-479	185	14	ring	ring	NOUN
eurjchem-479	186	1	[	[	X
eurjchem-479	186	2	16‐18	16‐18	NOUN
eurjchem-479	186	3	]	]	PUNCT
eurjchem-479	186	4	.	.	PUNCT
eurjchem-479	187	1	the	the	DET
eurjchem-479	187	2	activity	activity	NOUN
eurjchem-479	187	3	of	of	ADP
eurjchem-479	187	4	compound	compound	NOUN
eurjchem-479	187	5	7	7	NUM
eurjchem-479	187	6	against	against	ADP
eurjchem-479	187	7	all	all	DET
eurjchem-479	187	8	microorganisms	microorganism	NOUN
eurjchem-479	187	9	tested	test	VERB
eurjchem-479	187	10	showed	show	VERB
eurjchem-479	187	11	positive	positive	ADJ
eurjchem-479	187	12	reactions	reaction	NOUN
eurjchem-479	187	13	as	as	SCONJ
eurjchem-479	187	14	indicated	indicate	VERB
eurjchem-479	187	15	by	by	ADP
eurjchem-479	187	16	zone	zone	NOUN
eurjchem-479	187	17	of	of	ADP
eurjchem-479	187	18	inhibition	inhibition	NOUN
eurjchem-479	187	19	7	7	NUM
eurjchem-479	187	20	,	,	PUNCT
eurjchem-479	187	21	9	9	NUM
eurjchem-479	187	22	,	,	PUNCT
eurjchem-479	187	23	18	18	NUM
eurjchem-479	187	24	,	,	PUNCT
eurjchem-479	187	25	10	10	NUM
eurjchem-479	187	26	mm	mm	NOUN
eurjchem-479	187	27	,	,	PUNCT
eurjchem-479	187	28	respectively	respectively	ADV
eurjchem-479	187	29	,	,	PUNCT
eurjchem-479	187	30	this	this	PRON
eurjchem-479	187	31	may	may	AUX
eurjchem-479	187	32	be	be	AUX
eurjchem-479	187	33	due	due	ADJ
eurjchem-479	187	34	to	to	ADP
eurjchem-479	187	35	and	and	CCONJ
eurjchem-479	187	36	five	five	NUM
eurjchem-479	187	37	chlorine	chlorine	NOUN
eurjchem-479	187	38	atoms	atom	NOUN
eurjchem-479	187	39	,	,	PUNCT
eurjchem-479	187	40	respectively	respectively	ADV
eurjchem-479	187	41	.	.	PUNCT
eurjchem-479	188	1	the	the	DET
eurjchem-479	188	2	compound	compound	NOUN
eurjchem-479	188	3	8a	8a	NUM
eurjchem-479	188	4	showed	show	VERB
eurjchem-479	188	5	the	the	DET
eurjchem-479	188	6	most	most	ADJ
eurjchem-479	188	7	activity	activity	NOUN
eurjchem-479	188	8	against	against	ADP
eurjchem-479	188	9	bacteria	bacteria	NOUN
eurjchem-479	188	10	such	such	ADJ
eurjchem-479	188	11	as	as	ADP
eurjchem-479	188	12	bacillus	bacillus	NOUN
eurjchem-479	188	13	subtilis	subtili	NOUN
eurjchem-479	188	14	(	(	PUNCT
eurjchem-479	188	15	29	29	NUM
eurjchem-479	188	16	mm	mm	NOUN
eurjchem-479	188	17	)	)	PUNCT
eurjchem-479	188	18	which	which	PRON
eurjchem-479	188	19	is	be	AUX
eurjchem-479	188	20	2	2	NUM
eurjchem-479	188	21	mm	mm	NOUN
eurjchem-479	188	22	more	more	ADJ
eurjchem-479	188	23	than	than	ADP
eurjchem-479	188	24	the	the	DET
eurjchem-479	188	25	zone	zone	NOUN
eurjchem-479	188	26	around	around	ADP
eurjchem-479	188	27	tetracycline	tetracycline	PROPN
eurjchem-479	188	28	disc	disc	NOUN
eurjchem-479	188	29	(	(	PUNCT
eurjchem-479	188	30	27	27	NUM
eurjchem-479	188	31	mm	mm	NOUN
eurjchem-479	188	32	)	)	PUNCT
eurjchem-479	188	33	;	;	PUNCT
eurjchem-479	188	34	this	this	PRON
eurjchem-479	188	35	may	may	AUX
eurjchem-479	188	36	be	be	AUX
eurjchem-479	188	37	due	due	ADJ
eurjchem-479	188	38	to	to	ADP
eurjchem-479	188	39	presence	presence	NOUN
eurjchem-479	188	40	of	of	ADP
eurjchem-479	188	41	(	(	PUNCT
eurjchem-479	188	42	hn‐co‐ph	hn‐co‐ph	NOUN
eurjchem-479	188	43	)	)	PUNCT
eurjchem-479	188	44	.	.	PUNCT
eurjchem-479	189	1	the	the	DET
eurjchem-479	189	2	compound	compound	PROPN
eurjchem-479	189	3	8b	8b	PROPN
eurjchem-479	189	4	has	have	VERB
eurjchem-479	189	5	antimicrobial	antimicrobial	ADJ
eurjchem-479	189	6	effect	effect	NOUN
eurjchem-479	189	7	due	due	ADP
eurjchem-479	189	8	to	to	ADP
eurjchem-479	189	9	presence	presence	NOUN
eurjchem-479	189	10	of	of	ADP
eurjchem-479	189	11	bromine	bromine	NOUN
eurjchem-479	189	12	atom	atom	NOUN
eurjchem-479	189	13	[	[	X
eurjchem-479	189	14	19	19	NUM
eurjchem-479	189	15	]	]	PUNCT
eurjchem-479	189	16	.	.	PUNCT
eurjchem-479	190	1	the	the	DET
eurjchem-479	190	2	compound	compound	NOUN
eurjchem-479	190	3	9b	9b	NOUN
eurjchem-479	190	4	has	have	VERB
eurjchem-479	190	5	antimicrobial	antimicrobial	ADJ
eurjchem-479	190	6	effect	effect	NOUN
eurjchem-479	190	7	due	due	ADP
eurjchem-479	190	8	to	to	ADP
eurjchem-479	190	9	presence	presence	NOUN
eurjchem-479	190	10	of	of	ADP
eurjchem-479	190	11	(	(	PUNCT
eurjchem-479	190	12	no2	no2	NOUN
eurjchem-479	190	13	)	)	PUNCT
eurjchem-479	190	14	group	group	NOUN
eurjchem-479	190	15	.	.	PUNCT
eurjchem-479	191	1	the	the	DET
eurjchem-479	191	2	compounds	compound	NOUN
eurjchem-479	191	3	9d	9d	NOUN
eurjchem-479	191	4	and	and	CCONJ
eurjchem-479	191	5	10	10	NUM
eurjchem-479	191	6	showed	show	VERB
eurjchem-479	191	7	most	most	ADJ
eurjchem-479	191	8	activity	activity	NOUN
eurjchem-479	191	9	against	against	ADP
eurjchem-479	191	10	bacillus	bacillus	NOUN
eurjchem-479	191	11	subtilis	subtili	NOUN
eurjchem-479	191	12	(	(	PUNCT
eurjchem-479	191	13	18	18	NUM
eurjchem-479	191	14	mm	mm	NOUN
eurjchem-479	191	15	and	and	CCONJ
eurjchem-479	191	16	19	19	NUM
eurjchem-479	191	17	mm	mm	NOUN
eurjchem-479	191	18	,	,	PUNCT
eurjchem-479	191	19	respectively	respectively	ADV
eurjchem-479	191	20	)	)	PUNCT
eurjchem-479	191	21	.	.	PUNCT
eurjchem-479	192	1	this	this	PRON
eurjchem-479	192	2	may	may	AUX
eurjchem-479	192	3	be	be	AUX
eurjchem-479	192	4	due	due	ADJ
eurjchem-479	192	5	presence	presence	NOUN
eurjchem-479	192	6	of	of	ADP
eurjchem-479	192	7	(	(	PUNCT
eurjchem-479	192	8	hn‐co	hn‐co	NOUN
eurjchem-479	192	9	)	)	PUNCT
eurjchem-479	192	10	group	group	NOUN
eurjchem-479	192	11	in	in	ADP
eurjchem-479	192	12	two	two	NUM
eurjchem-479	192	13	compounds	compound	NOUN
eurjchem-479	192	14	.	.	PUNCT
eurjchem-479	193	1	scheme	scheme	NOUN
eurjchem-479	193	2	6	6	NUM
eurjchem-479	193	3	acknowledgements	acknowledgement	NOUN
eurjchem-479	193	4	the	the	DET
eurjchem-479	193	5	authors	author	NOUN
eurjchem-479	193	6	are	be	AUX
eurjchem-479	193	7	grateful	grateful	ADJ
eurjchem-479	193	8	to	to	ADP
eurjchem-479	193	9	dr	dr	PROPN
eurjchem-479	193	10	.	.	PROPN
eurjchem-479	193	11	yousif	yousif	PROPN
eurjchem-479	193	12	hassn	hassn	PROPN
eurjchem-479	193	13	ebied	ebie	VERB
eurjchem-479	193	14	for	for	ADP
eurjchem-479	193	15	his	his	PRON
eurjchem-479	193	16	help	help	NOUN
eurjchem-479	193	17	.	.	PUNCT
eurjchem-479	194	1	references	reference	NOUN
eurjchem-479	194	2	[	[	X
eurjchem-479	194	3	1	1	NUM
eurjchem-479	194	4	]	]	PUNCT
eurjchem-479	194	5	.	.	PUNCT
eurjchem-479	195	1	agrawal	agrawal	PROPN
eurjchem-479	195	2	,	,	PUNCT
eurjchem-479	195	3	j.	j.	PROPN
eurjchem-479	195	4	p.	p.	PROPN
eurjchem-479	195	5	;	;	PUNCT
eurjchem-479	195	6	chouk	chouk	PROPN
eurjchem-479	195	7	m.	m.	NOUN
eurjchem-479	195	8	p.	p.	NOUN
eurjchem-479	195	9	res	re	NOUN
eurjchem-479	195	10	.	.	PUNCT
eurjchem-479	196	1	ind	ind	PROPN
eurjchem-479	196	2	.	.	PUNCT
eurjchem-479	197	1	j.	j.	PROPN
eurjchem-479	197	2	1982	1982	NUM
eurjchem-479	197	3	,	,	PUNCT
eurjchem-479	197	4	27	27	NUM
eurjchem-479	197	5	,	,	PUNCT
eurjchem-479	197	6	19‐21	19‐21	NUM
eurjchem-479	197	7	.	.	PUNCT
eurjchem-479	198	1	[	[	X
eurjchem-479	198	2	2	2	NUM
eurjchem-479	198	3	]	]	PUNCT
eurjchem-479	198	4	.	.	PUNCT
eurjchem-479	199	1	sou	sou	PROPN
eurjchem-479	199	2	,	,	PUNCT
eurjchem-479	199	3	s.	s.	PROPN
eurjchem-479	199	4	;	;	PUNCT
eurjchem-479	199	5	mayumi	mayumi	PROPN
eurjchem-479	199	6	,	,	PUNCT
eurjchem-479	199	7	s.	s.	PROPN
eurjchem-479	199	8	;	;	PUNCT
eurjchem-479	199	9	takahashi	takahashi	PROPN
eurjchem-479	199	10	,	,	PUNCT
eurjchem-479	199	11	h.	h.	PROPN
eurjchem-479	199	12	;	;	PUNCT
eurjchem-479	199	13	yamasaki	yamasaki	PROPN
eurjchem-479	199	14	,	,	PUNCT
eurjchem-479	199	15	r.	r.	PROPN
eurjchem-479	199	16	;	;	PUNCT
eurjchem-479	199	17	kadoya	kadoya	PROPN
eurjchem-479	199	18	,	,	PUNCT
eurjchem-479	199	19	s.	s.	PROPN
eurjchem-479	199	20	;	;	PUNCT
eurjchem-479	199	21	sodeoka	sodeoka	NOUN
eurjchem-479	199	22	,	,	PUNCT
eurjchem-479	199	23	m.	m.	NOUN
eurjchem-479	199	24	;	;	PUNCT
eurjchem-479	199	25	hashimoto	hashimoto	NOUN
eurjchem-479	199	26	,	,	PUNCT
eurjchem-479	199	27	y.	y.	PROPN
eurjchem-479	199	28	bioorg	bioorg	PROPN
eurjchem-479	199	29	.	.	PUNCT
eurjchem-479	200	1	med	med	PROPN
eurjchem-479	200	2	.	.	PROPN
eurjchem-479	200	3	chem	chem	PROPN
eurjchem-479	200	4	.	.	PUNCT
eurjchem-479	201	1	lett	lett	PROPN
eurjchem-479	201	2	.	.	PROPN
eurjchem-479	201	3	2000	2000	NUM
eurjchem-479	201	4	,	,	PUNCT
eurjchem-479	201	5	10	10	NUM
eurjchem-479	201	6	,	,	PUNCT
eurjchem-479	201	7	1081‐1086	1081‐1086	NUM
eurjchem-479	201	8	.	.	PUNCT
eurjchem-479	202	1	[	[	X
eurjchem-479	202	2	3	3	NUM
eurjchem-479	202	3	]	]	PUNCT
eurjchem-479	202	4	.	.	PUNCT
eurjchem-479	203	1	valencia	valencia	PROPN
eurjchem-479	203	2	,	,	PUNCT
eurjchem-479	203	3	r.	r.	PROPN
eurjchem-479	203	4	;	;	PUNCT
eurjchem-479	203	5	mason	mason	PROPN
eurjchem-479	203	6	m.	m.	PROPN
eurjchem-479	203	7	j.	j.	PROPN
eurjchem-479	203	8	;	;	PUNCT
eurjchem-479	203	9	woodruff	woodruff	PROPN
eurjchem-479	203	10	c.	c.	PROPN
eurjchem-479	203	11	r.	r.	PROPN
eurjchem-479	203	12	;	;	PUNCT
eurjchem-479	203	13	zimmering	zimmering	NOUN
eurjchem-479	203	14	,	,	PUNCT
eurjchem-479	203	15	s.	s.	PROPN
eurjchem-479	203	16	environ	environ	PROPN
eurjchem-479	203	17	.	.	PUNCT
eurjchem-479	204	1	mutagen	mutagen	PROPN
eurjchem-479	204	2	.	.	PROPN
eurjchem-479	205	1	1985	1985	NUM
eurjchem-479	205	2	,	,	PUNCT
eurjchem-479	205	3	7	7	NUM
eurjchem-479	205	4	,	,	PUNCT
eurjchem-479	205	5	325‐348	325‐348	NUM
eurjchem-479	205	6	.	.	PUNCT
eurjchem-479	206	1	[	[	X
eurjchem-479	206	2	4	4	NUM
eurjchem-479	206	3	]	]	PUNCT
eurjchem-479	206	4	.	.	PUNCT
eurjchem-479	206	5	wenzel	wenzel	PROPN
eurjchem-479	206	6	,	,	PUNCT
eurjchem-479	206	7	d.	d.	PROPN
eurjchem-479	206	8	g.	g.	PROPN
eurjchem-479	206	9	j.	j.	PROPN
eurjchem-479	206	10	am	am	PROPN
eurjchem-479	206	11	.	.	PUNCT
eurjchem-479	207	1	pharm	pharm	PROPN
eurjchem-479	207	2	.	.	PUNCT
eurjchem-479	208	1	assoc	assoc	PROPN
eurjchem-479	208	2	.	.	PUNCT
eurjchem-479	209	1	1995	1995	NUM
eurjchem-479	209	2	,	,	PUNCT
eurjchem-479	209	3	44	44	NUM
eurjchem-479	209	4	,	,	PUNCT
eurjchem-479	209	5	550‐553	550‐553	NUM
eurjchem-479	209	6	.	.	PUNCT
eurjchem-479	210	1	[	[	X
eurjchem-479	210	2	5	5	NUM
eurjchem-479	210	3	]	]	PUNCT
eurjchem-479	210	4	.	.	PUNCT
eurjchem-479	211	1	hansen	hansen	PROPN
eurjchem-479	211	2	,	,	PUNCT
eurjchem-479	211	3	p.	p.	PROPN
eurjchem-479	211	4	;	;	PUNCT
eurjchem-479	211	5	pederesen	pederesen	PROPN
eurjchem-479	211	6	,	,	PUNCT
eurjchem-479	211	7	e.	e.	PROPN
eurjchem-479	211	8	b.	b.	PROPN
eurjchem-479	211	9	acta	acta	PROPN
eurjchem-479	211	10	chem	chem	PROPN
eurjchem-479	211	11	.	.	PUNCT
eurjchem-479	212	1	scand	scand	PROPN
eurjchem-479	212	2	.	.	PUNCT
eurjchem-479	213	1	1990	1990	NUM
eurjchem-479	213	2	,	,	PUNCT
eurjchem-479	213	3	44	44	NUM
eurjchem-479	213	4	,	,	PUNCT
eurjchem-479	213	5	522‐523	522‐523	NUM
eurjchem-479	213	6	.	.	PUNCT
eurjchem-479	214	1	[	[	X
eurjchem-479	214	2	6	6	NUM
eurjchem-479	214	3	]	]	PUNCT
eurjchem-479	214	4	.	.	PUNCT
eurjchem-479	215	1	maillard	maillard	NOUN
eurjchem-479	215	2	,	,	PUNCT
eurjchem-479	215	3	j.	j.	PROPN
eurjchem-479	215	4	;	;	PUNCT
eurjchem-479	215	5	vincent	vincent	PROPN
eurjchem-479	215	6	m.	m.	NOUN
eurjchem-479	215	7	;	;	PUNCT
eurjchem-479	215	8	benard	benard	NOUN
eurjchem-479	215	9	,	,	PUNCT
eurjchem-479	215	10	m.	m.	NOUN
eurjchem-479	215	11	chem	chem	PROPN
eurjchem-479	215	12	.	.	PUNCT
eurjchem-479	216	1	ther	ther	PROPN
eurjchem-479	216	2	.	.	PUNCT
eurjchem-479	217	1	1968	1968	NUM
eurjchem-479	217	2	,	,	PUNCT
eurjchem-479	217	3	3	3	NUM
eurjchem-479	217	4	,	,	PUNCT
eurjchem-479	217	5	100‐106	100‐106	NUM
eurjchem-479	217	6	.	.	PUNCT
eurjchem-479	218	1	[	[	X
eurjchem-479	218	2	7	7	NUM
eurjchem-479	218	3	]	]	PUNCT
eurjchem-479	218	4	.	.	PUNCT
eurjchem-479	219	1	hong	hong	PROPN
eurjchem-479	219	2	,	,	PUNCT
eurjchem-479	219	3	e.	e.	PROPN
eurjchem-479	219	4	u.	u.	PROPN
eurjchem-479	219	5	s.	s.	PROPN
eurjchem-479	219	6	patent	patent	PROPN
eurjchem-479	219	7	3726979	3726979	NUM
eurjchem-479	219	8	.	.	PUNCT
eurjchem-479	220	1	chem	chem	NOUN
eurjchem-479	220	2	.	.	PUNCT
eurjchem-479	221	1	abstract	abstract	ADJ
eurjchem-479	221	2	.	.	PUNCT
eurjchem-479	222	1	1973	1973	NUM
eurjchem-479	222	2	,	,	PUNCT
eurjchem-479	222	3	79	79	NUM
eurjchem-479	222	4	,	,	PUNCT
eurjchem-479	222	5	27560a	27560a	NUM
eurjchem-479	222	6	.	.	PUNCT
eurjchem-479	223	1	[	[	X
eurjchem-479	223	2	8	8	NUM
eurjchem-479	223	3	]	]	PUNCT
eurjchem-479	223	4	.	.	PUNCT
eurjchem-479	224	1	akgun	akgun	PROPN
eurjchem-479	224	2	,	,	PUNCT
eurjchem-479	224	3	h.	h.	PROPN
eurjchem-479	224	4	;	;	PUNCT
eurjchem-479	224	5	hollstein	hollstein	ADV
eurjchem-479	224	6	,	,	PUNCT
eurjchem-479	224	7	u.	u.	PROPN
eurjchem-479	224	8	;	;	PUNCT
eurjchem-479	224	9	hrwitz	hrwitz	PROPN
eurjchem-479	224	10	l.	l.	PROPN
eurjchem-479	224	11	j.	j.	PROPN
eurjchem-479	224	12	pharm	pharm	PROPN
eurjchem-479	224	13	.	.	PUNCT
eurjchem-479	225	1	sci	sci	PROPN
eurjchem-479	225	2	.	.	PROPN
eurjchem-479	225	3	1988	1988	NUM
eurjchem-479	225	4	,	,	PUNCT
eurjchem-479	225	5	77	77	NUM
eurjchem-479	225	6	,	,	PUNCT
eurjchem-479	225	7	735‐739	735‐739	NUM
eurjchem-479	225	8	.	.	PUNCT
eurjchem-479	226	1	[	[	X
eurjchem-479	226	2	9	9	NUM
eurjchem-479	226	3	]	]	PUNCT
eurjchem-479	226	4	.	.	PUNCT
eurjchem-479	226	5	havera	havera	PROPN
eurjchem-479	226	6	,	,	PUNCT
eurjchem-479	226	7	h.	h.	PROPN
eurjchem-479	226	8	j.	j.	PROPN
eurjchem-479	226	9	;	;	PUNCT
eurjchem-479	226	10	vidiro	vidiro	PROPN
eurjchem-479	226	11	h.	h.	PROPN
eurjchem-479	226	12	j.	j.	PROPN
eurjchem-479	226	13	med	med	PROPN
eurjchem-479	226	14	.	.	PROPN
eurjchem-479	226	15	chem	chem	PROPN
eurjchem-479	226	16	.	.	PUNCT
eurjchem-479	227	1	1979	1979	NUM
eurjchem-479	227	2	,	,	PUNCT
eurjchem-479	227	3	22	22	NUM
eurjchem-479	227	4	,	,	PUNCT
eurjchem-479	227	5	1548‐1550	1548‐1550	NUM
eurjchem-479	227	6	.	.	PUNCT
eurjchem-479	228	1	[	[	X
eurjchem-479	228	2	10	10	NUM
eurjchem-479	228	3	]	]	PUNCT
eurjchem-479	228	4	.	.	PUNCT
eurjchem-479	229	1	havera	havera	PROPN
eurjchem-479	229	2	h.	h.	PROPN
eurjchem-479	229	3	j.	j.	PROPN
eurjchem-479	229	4	ger	ger	PROPN
eurjchem-479	229	5	.	.	PUNCT
eurjchem-479	230	1	patent	patent	NOUN
eurjchem-479	230	2	242858	242858	NUM
eurjchem-479	230	3	,	,	PUNCT
eurjchem-479	230	4	(	(	PUNCT
eurjchem-479	230	5	1979	1979	NUM
eurjchem-479	230	6	)	)	PUNCT
eurjchem-479	230	7	.	.	PUNCT
eurjchem-479	231	1	chem	chem	NOUN
eurjchem-479	231	2	.	.	PUNCT
eurjchem-479	232	1	abstract	abstract	ADJ
eurjchem-479	232	2	1975	1975	NUM
eurjchem-479	232	3	,	,	PUNCT
eurjchem-479	232	4	82	82	NUM
eurjchem-479	232	5	,	,	PUNCT
eurjchem-479	232	6	171029p	171029p	NUM
eurjchem-479	232	7	.	.	PUNCT
eurjchem-479	233	1	[	[	X
eurjchem-479	233	2	11	11	NUM
eurjchem-479	233	3	]	]	PUNCT
eurjchem-479	233	4	.	.	PUNCT
eurjchem-479	234	1	fahmy	fahmy	PROPN
eurjchem-479	234	2	,	,	PUNCT
eurjchem-479	234	3	a.	a.	PROPN
eurjchem-479	234	4	f.	f.	PROPN
eurjchem-479	234	5	m.	m.	PROPN
eurjchem-479	234	6	;	;	PUNCT
eurjchem-479	234	7	youssef	youssef	PROPN
eurjchem-479	234	8	,	,	PUNCT
eurjchem-479	234	9	m.	m.	NOUN
eurjchem-479	234	10	s.	s.	PROPN
eurjchem-479	234	11	k.	k.	PROPN
eurjchem-479	234	12	;	;	PUNCT
eurjchem-479	234	13	abdel	abdel	PROPN
eurjchem-479	234	14	halim	halim	PROPN
eurjchem-479	234	15	,	,	PUNCT
eurjchem-479	234	16	m.	m.	NOUN
eurjchem-479	234	17	s.	s.	PROPN
eurjchem-479	234	18	;	;	PUNCT
eurjchem-479	234	19	hassan	hassan	PROPN
eurjchem-479	234	20	m.	m.	PROPN
eurjchem-479	234	21	a.	a.	PROPN
eurjchem-479	234	22	;	;	PUNCT
eurjchem-479	234	23	saur	saur	PROPN
eurjchem-479	234	24	,	,	PUNCT
eurjchem-479	234	25	j.	j.	PROPN
eurjchem-479	234	26	heterocycles	heterocycles	PROPN
eurjchem-479	234	27	1986	1986	NUM
eurjchem-479	234	28	,	,	PUNCT
eurjchem-479	234	29	24	24	NUM
eurjchem-479	234	30	,	,	PUNCT
eurjchem-479	234	31	2201‐2213	2201‐2213	NUM
eurjchem-479	234	32	.	.	PUNCT
eurjchem-479	235	1	[	[	X
eurjchem-479	235	2	12	12	NUM
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eurjchem-479	238	2	.	.	PUNCT
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eurjchem-479	240	3	]	]	PUNCT
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eurjchem-479	246	4	.	.	PUNCT
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eurjchem-479	248	2	,	,	PUNCT
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eurjchem-479	248	6	.	.	PUNCT
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eurjchem-479	249	4	.	.	PUNCT
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eurjchem-479	250	2	,	,	PUNCT
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eurjchem-479	251	4	.	.	PUNCT
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eurjchem-479	252	2	,	,	PUNCT
eurjchem-479	252	3	6	6	NUM
eurjchem-479	252	4	,	,	PUNCT
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eurjchem-479	252	6	.	.	PUNCT
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eurjchem-479	253	4	.	.	PUNCT
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eurjchem-479	254	10	l.	l.	PROPN
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eurjchem-479	255	4	.	.	PUNCT
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eurjchem-479	257	3	.	.	PUNCT
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eurjchem-479	258	2	,	,	PUNCT
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